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-------
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-------
                                             _.7lRO'.-_JTAL _fclNL_.jNG,' ...I.
                                                  Gainesville, Florida

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-------
GRAB SAMPLE COLLECTION

-------
               Mo.
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                        7S"
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-------
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-------
avtl
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              Wo.
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                                               Z,
 fluorides

-------
EPA
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        AUtals

-------
                                5Z
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-------
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-------
           APPENDIX C
Standard Analytical Procedures

-------
                         ENVIRONMENTAL PROTECTION AGENCY

             .  .      Research Triangle Park,  North Carolina   27711

Reply to

 Atln °J:                                     '                       •  Dau:  12-21-72

 Subject:  summary of Fluoride Analysis


   T" »                                                                       •
     '   R: Neulicht,  EMB,  IRL             .                      •
           • This memorandum is  in  response  to your request for  a brief
        summary  of  our SPADNS-Zirconium Lake procedure  for  determination
        of  fluoride in stack emission  samples.

            Samples received in our laboratory are filtered through
        fluoride free paper  filters to yield water soluble  and water  insoluble
        portions.   The water insoluble particulate collected on  the filter
        is  rinsed throughly  to be sure that  all water soluble fluoride  is
        rinsed through.  The water  soluble fraction is  distilled from sul-
        furic acid  to a maximum  temperature  of  180 C.    If  chloride is  suspected
        in  the sample Ag So. is  added  to the still.  SPADNS solution  is added
        to  an aliquot of the distillate and  the absorbance  is read at 570 nm.
        The concentration of the sample is determined from  a calibration curve
        prepared from standard fluoride solutions.   It  is very important that
        the temperature of the samples be the same as that  of the standards
        when absorbances are recorded.

            The water insoluble fraction of the sample is  evaporated to dry-
        ness in  the presence of  a slurry or  
-------
     APPENDIX E
Project Participants

-------
                        PROJECT PARTICIPANTS

      Name                              ,                 Titl e
John Dollar                                    Project Manager
George Allen                                   Environmental  Specialist
Ray Black        %                              Environmental  Specialist
John Cutts                                     Environmental  Specialist
Bob Durgan                                     Environmental  Specialist
Dennis Falgout                                 Environmental  Specialist
Albert Henderson                               Environmental  Specialist
Tom Tucker -, :  .                               Environmental  Specialist
Larry Hurts                                    Environmental  Specialist
Jerome Rom                                     EPA
John Reynolds                                  EPA
Roy Neulicht                                   EPA

-------

                       72 - CI - 5B
                   BORDEN CHEMICAL, INC.
          GRANULAR TRIPLE SUPERPHOSPHATE STORAGE
                      PINEY POINT
                    JANUARY 24, 1972
                  enrironmvntal
2324 S. W. 34th STREET / GAINESVILLE, FLORIDA  32601  / PHONE 904/372-3318

-------
              72 - CI - 5B
          BORDEN CHEMICAL, INC.
GRANULAR TRIPLE SUPERPHOSPHATE STORAGE                                 ji
             .PINEY POINT         .'•                                    [I
           JANUARY 24, 1972                                            !
           Test Conducted by:
    Environmental Engineering, Inc.
        Contract # CPA 70 - 82

-------
                          TABLE OF CONTENTS
                                                        Page
List of Figures                                          ii
List of Tables                                           iii
Introduction                                              1
Summary of Results                                  .1
Process Description                                       5
Process Operation                                         5
Location of Sampling Points                               6
Sampling and Analytical Procedures                        9
Appendix                                                 13
  A.  Emission Calculations and Results
  B.  Field Data
  C.  Standard Analytical Procedures
  D.  Laboratory Results
  E.  Project Participants
                             1i

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\
                              LIST OF FIGURES
                                                        Page
     1.  Schematic Flow Diagram                           2
     2.  Sample Port Location - Scrubber Outlet           7
     3.  Sample Port Location - Scrubber Inlet            8
     4.  Fluoride Sampling Train                         10

                              LIST OF TABLES
     1.  Summary of Results - Scrubber Outlet             3
     2.  Summary of Results - Scrubber Inlet              4
                                  iii

-------
INTRODUCTION
     Under the direction of the Environmental  Protection Agency,  Environ-
mental Engineering, Inc. conducted emission tests at the Borden Chemical,
Inc. phosphate works 1n P1ney Point, Florida.   On January 24,  1972, three
test runs of approximately eighty minutes each were conducted  on  Borden's
granular triple superphosphate storage building.  The purpose  of  the tests
was to obtain emission data for the use of both the Industrial  Studies
Branch and the Performance Standards Branch of the EPA.

     Measurements for total fluorides were made at the inlet and  outlet
ducts of the storage off-gas scrubber.  Grab samples of the scrubbing liquid
were taken during the test runs and analyzed for fluoride content.   A schema-
tic flow diagram of the process operation and  the sampling locations is given
in Figure 1.  Complete test results are given  in Appendix A.
                                                                  %
SUMMARY OF RESULTS

     The amount of granular triple superphosphate located in storage during
the test runs was approximately 1400 tons P2°5'  Loading of the product into
rail cars was taking place during the test runs.
     No major problems were encountered during the sampling; the  only irregu-
larity occurred at the scrubber outlet.  At the first three traverse points of
the duct the gas flow was negative.  For this  reason, although the  true duct
                2                                                          2
area was 26.3 FT , the effective stack area was calculated to  be  only 23 FT .
The value for the effective stack area was used In all calculations.
  \
     A complete summary of the stack conditions and fluoride concentrations for
each test point 1s given 1n Tables 1 and 2.

-------
   GTSP Product
Storage
-Q-
                                        Pond Water
                                             I
Tail Gas
Scrubber
                                                       T
                                                     To Pond
                                                                               To
                                                                           Atmosphere
                                                                             Stack
                                   FIGURE 1
                                 GTSP STORAGE
                            BORDEN CHEMICAL,  INC.

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                                TABLE  1
                          SUMMARY  OF  RESULTS
                               FLUORIDES

                          "Scrubber Outlet  •-
Run No.
Date
Barometric pressure, inches Hg
5."ack pressure, inches Hg
Stack gas moisture, % volume
A- erage stack gas temperature, °F.
Stack gas flow rate @ S.T.P., SCFM
Vol. dry gas G> S.T.P. , SCF
Fluoride, water soluble, mg
i
Fluoride, total , mg
Fluoride, water soluble, gr/SCF
Fluoride, total , gr/SCF
Fluoride, water soluble, gr/CF stk. cond.
Fluoride, total, gr/CF stk. cond.
Fluoride, water soluble, Ib/hour
Fluoride, total, Ib/hour
Product in Storage, Tons P2®5
Fluoride, water soluble, (lb/hr)/ton
P?05 stored
Fluoride, total (lb/hr)/ton PoOc
stored. c °
Scrubber efficiency, %
1
1-24-72
30
30
2.3 '
75
64844
81.9
5.6
5.61
0.0011
0.0011
0.001
0.001
0.61
.0.61
1430
0;0004
0.0004
71.6
2
1-24-72
30
30
2.3
75
64401
79.439
4.1 ,
4.133
0.0008
0.0008
0.0008
0.0008
0.44
0.44
1430
\
0.0003
0.0003
54.2
3
1-24-72
30
30
2.2
75
65744
82.663
4.6
4.687
0.0009
0.0009
0.0008
'0.0008
0.51
0.51
1430
0.0003
0.0003
71.5
Dry, 70°F., 29.92 inches  Hg.

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                                TABLE 2
                          SUMMARY OF RESULTS
                               FLUORIDES

                         '•• : SCRUBBER INLET
Run No.
Date
Barometric pressure, inches Hg
Stack pressure, inches He.
Stack gas moisture, % volume
Average stack gas temper? iMre, 'T.
Stack gas flow rate @ S.T.P., SCFM
Vol. dry gas @ S.T.P. , SCF
Fluoride, water soluble, mg
Fluoride, total , mg
Fluoride, water soluble, gr/SCF
Fluoride, total, gr/SCF
Fluoride, water soluble, gr/CF stk. cond.
Fluoride, total, gr/CF stk. cond.
Fluoride, water soluble, Ib/hour
Fluoride, total, Ib/hour
Product in Storage, Tons P205
Fluoride, water soluble, (lb/hr.)/ton
P^05 stored ' - . .
Ftuoride, total, (lb/hr)/ton
PoOi- stored
*• j
Scrubber efficiency, %
I
1-24-72
30
29.75
0.5
85
83457
84.432
16.3
16.59
0.003
0.003
0.0029
0.0029
2,. 15
2. 15
1430
0.0015
0.0015
-
2
1-24-72
30
29.75
0.4
85
. 79621
91.941
8.3 ,
8.44
Q.0014
0.0014
0.0013
0.0014
0,96
0,96
1430
0.0007
0.0007
-
3
1-24-72
30
29.75
0.9
84
74427
84.934
15.3
15.372
0.0028
0.0028
0.0027
0.0027
1..79
1.79
1430
0.0012
0.0012
-
Dry, 70°F., 29.92 inches Hg.

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PROCESS DESCRIPTION

     Bulk granular triple superphosphate is stored 1n a large building.
Emissions generated by the curing, and the handling of the product while
loading on rail cars are vented to a packed scrubber.

PROCESS OPERATION

     Operating conditions were normal  during all  three test runs.
                                             \

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LOCATION OF SAMPLING POINTS

          The sampling sites and number of "traverse points were
selected as per "Method I - Sample and Velocity Traverses for Sta-
tionary Sources, Part 60, Subchapter C, Chapter 1,  Title 40," Federal
Register, No. 247-Pt. II-l.
          The above method suggests using two perpendicular diameters
of traverse points per sampling station, however, on-site conditions
necessitated the use of only one traverse diameter.  The suggested
number of traverse points per diameter was used where possible without
sampling within one inch of the inner wall.
          Figures 2 through 3 are schematic diagrams of the stack
configurations near the sampling location, and the sampling points
traversed during the emission tests.

-------
         Top View
Side View
Traverse Point
     1
     2
     3
     4
     5
     6
     7
     8
     9
    10
    11
    12
    13
    14
    15
    16
    17   '
    18
    19
    20
    21
    22
    23
    24
Distance from
Inner Wall (in.)
     1
     3
     5
     7
     9
    11
    13
    15
    17
    19
    21
    23
    25
    27
    29
    31
    33
    35
    37
    39
    41
    43
 -   45
    47
                    FIGURE 2

  LOCATION OF PORT, STATION Q, BORDEN CHEMICALS

                 SCRUBBER OUTLET

-------
           35'
	 e»

N
, >
•a— 12' — B*
i
* — 12' 	 »•

x° ^
' t- Port


Scrubber


                 Damper

                   Diameter = 5.5 ft
Traverse Point

      1
      2
      3
      4
      5
      6
      7
      8
Distance from Inner Wall (in.)

           2 ,3/16
           6 15/16
          12 13/16
          21  3/8
          44  5/8
          53  1/4
          59  1/8
          63 15/16
                 FIGURE 3

LOCATION OF PORT, STATION P, BORDEN CHEMICALS

             SCRUBBER INLET-
                  8

-------
SAMPLING AND ANALYTICAL PROCEDURES
A.  Preliminary Moisture Determination
          The preliminary moisture contents were determined from wet
and dry bulb thermometry. See Appendix B for the data used in deter-
mining the preliminary moisture content of the stack gases.
          The final moisture content was determined as per Method 5
of the Federal Register (Volume 36* Number 297, Paragraph II, December
23, 1971) by totalling the condensate collected in the three impingers
and the silica gel.
B.  Preliminary Velocity Determination
          Method 2 of the above mentioned Federal Register was used
as a guide in determining the preliminary stack gas velocity for each
source tested.  The major difference was that only the maximum and
minimum velocity heads across each stack area were determined so that
a proper nozzle size could be selected.  During each of the three fluoride
emission tests, velocity head readings were taken at points selected
by using Method 1 of the Federal Register.
          Stack pressure and temperature measurements were also made
during the preliminary velocity determinations.
C.  Sampling for Fluoride Emissions
          The sampling procedure used for determining fluoride emissions
was similar to Method 5 of the Federal Register.  The major difference
between the two methods wastthe configuration o"f the sampling train.  The
sampling train described in the Federal Register has a heated box con-
taining the filter holder directly following the glass probe.  The s

-------
100 ml
100 ml
   1.   Stainless Steel  Nozzle
   2.   Heated Glass  Probe
   3.   Glass Connector
   4.   Ice Bath
   5.   Impinger with
   6.   Impinger with
   7.   Impinger, Dry
   8.   Impinger with
   9.   Filter Holder
  10.   Thermometer
_n.   Flexible Sample  Line
o!2.   Vacuum Gauge
  13.   Main Control  Valve
  14.   By-Pass Control  Valve
  15.   Air Tight Vacuum Pump
  16.   Dry Test Meter
  17.   Calibrated Orifice
  13.   Inclined Manometer
  19.   S-Type Pi tot  Tube
H90
H0
                    19
(Modified Tip)
             )
           (Standard Tip
(Modified Tip)
180 grams Silica Gel (Modified Tip)
with No. 1 Whatman Filter
                     17
                                    Figure  4

                              FLUORIDE SAMPLING' TRAIN .

-------
sampling train used in these tests contained no heated box and the filter
holder was placed between the third and fourth'impingers (between dry
impinger and silica gel impinger).to prevent sample carryover.   Figure  4
is a schematic diagram of the sampling train used.
           After the selection of the sampling site and the minimum number
of sampling points per Method 2 of the above mentioned Federal Register,
three separate test runs were performed.  For each run, the required
stack and sampling parameters were recorded on field data sheets.  They
are included in Appendix B>.  Readings were taken at each traverse point
at least every five minutes, and when significant changes in stack para-
meters necessitated additional adjustments to maintain an isokinetic flow
rate.  Nomographs were used to aid in the rapid adjustment of the sampling
rate.  The traverse points were selected to maintain at least one inch
from the  inner stack wall.
                                            *
           After each  run, the liquid volume in the first three  impingers
was measured volumetrically and the silica gel was reweighed.  The im-
pinger liquid, the filter, plus the water washings of the probe  and other
sampling  train components up  to the silica  gel. were placed  into  a
single polyethylene container.
D.  Liquid and Product Grab Samples
          Periodically, during each test run, grab samples  of the raw
materials, finished product,  and  scrubber liquid were taken, and the
temperature and pH were determined at the site.
E.  Laboratory Analysis
          Water soluble fluorides were done by a sulfuric acid distil-
                                  n

-------
      lation followed by the SPADNS-ZIRCONIIM LAKE  METHOD.   Water insoluble
      fluorides  were first fused  with  NaOH  followed by a  sulfuric acid distil-
      lation then by the SPADNS-ZIRCONIUM LAKE METHOD.
                For more details  of exact method  used  see Appendix C.
\
                                       12

-------
APPENDIX
    13

-------
          APPENDIX A
Emission  Calculations & Results

-------
              E.E.I. SOURCE SAMPLING NOMENCLATURE SHEET
  PB - Barometric pressure, inches Hg
  PS - Stack pressure, inches Hg
  As - Stack area, sq. ft.
  AS1- Effective area of positive stack gas flow, sq. ft.
NPTS - Number of traverse points where the pitot velocity head was greater than zero,
  TS - Stack temperature, °R
  TM - Meter temperature, °R
  E  - Average square root of velocity head, Vinches H20
  AH - Average meter orifice pressure differential, inches ^0
  AN - Sampling nozzle area, square feet
  CP - S-type pitot tube correction factor
  VM - Recorded meter volume sample, cubic feet (meter conditions)
  VC - Condensate and silica gel increase in impringers, milliliters
  Po - Pressure at the dry test meter orifice, [PB +A. H~| inches Hg
                                               L   13.6J
 STP - Standard conditions, dry, 70°F, 29.92 inches Hg
       Conversion of condensate in milliliters to water vapor in cubic feet (STP)
       Volume sampled, cubic feet (STP)
       Total water vapor volume and dry gas volume sampled, cubic feet (STP)
       Moisture fraction of stack gas
       Dry gas fraction                       . .
       Molecular weight of stack gas, lbs/lb-mole (dry conditions)
       Molecular weight of stack gas, lbs/lb-mole (stack conditions)
       Specific gravity of stack gas, referred to air
       Excess air, %
       Average square root of velocity head times stack temperature
       Stack gas velocity, feet per minute
       Stack gas flow rate, cubic feet per minute (stack conditions)
       Stack gas flow rate, cubic feet per minute (dry conditions)
       Stack gas flow rate, cubic feet-per minute (STP)
       Percent isokinetic volume sampled (method described in Federal Register)
       Total sample time,  minutes

-------
              EQUATIONS FOR CALCULATING  FLUORIDE EMISSIONS










   VWV = (0.0474) x  (VC)




 VSTPD = (17 . 71 x (VM) x  (PB +  — B-  ) -=- TM

                                13.6


    VT = (VWV) + (VSTPD)




     W = (VWV)-j-(VT)




   FDA - (1.0) - (W)




FMOIST = Assumed moisture fraction




    MD = (0.44 x % CO  ) + (0.32 x % 02)  + (0.28 x % NZ) + (0.28 x % CO)




    MS = (MD x FDA)  +  (18 x W)




    GS = (MS) -h (28. 99)
                                                             ^



    EA =  [(100) x (% 02 - SjEO)] ~ [(0.266 x % NZ) - (% 02 - ^^)]




     U = (174) x (CP)  x  (H) x \ftTS x 29.92)-~(GS x PS)




    QS = (£) x  (AS)




    QD = (QS) x  (FDA)                                                      .




 QSTPD = (530) x (QD)-J-(TS)x (PS)  r  (29.92)




  PISO = Qo. oo267 x VC x TS) -f (PQ x TS x VM-5-TM)]  -7-  [(Time x U x PS x AN)]






Fluoride Emissions:




       MG = Milligrams of fluoride from lab analysis




       Grains/SCF =  (0.01543) x  (MG) -f- VSTPD




       Grains/CF, Stack Cond.  =  (17.71) x (PS) x (FDA) x (Grains/SCF) ~ (TS)




       Lbs/hour = (Grains/SCF) x  (0.00857) x (QSTPD)




                = Tons/hour, determined  from plant data
       Lbs/ton P20  Fed =  (Ibs/hour) -~ (Tons/hour -P205 Fed)

-------
FLUORIDE EMISSIONS

-------
    TEST  NO  -                            no OF nuns -
    PLANT -  BORDEN CHEMI-CAL    PINEY  POINT,  FLA.
    SOURCE - F/.ff.  SCRUPBER INLET
    TYPE  OF  PLANT -  FERTILIZER STORAGE
    CONTROL  EQUIPMENT -
    POLLUTANTS SAMPLED - FLUORIDES
DliUt! NUMBER
2 ) DA TE
3) TIME BEGAN
• *)TIME END
S)BAROMETRIC PRESSURE, IN JIG
&)METER ORIFICE PRESSURE DROP, IN HG
7) VOL DRY GAS, METER COND, CUBIC FEET
8) AVER AGE GAS METER TEMPERATURE, DEG F
Q)VOL DRY GAS, S.T.P. , CUBIC FEET
10) TOTAL U20 COLLECTED, ML
11) VOL 1120 VAPOR COLLECTED, S.T.P. , CU
12)STACK GAS MOISTURE, PERCENT VOLUME
13) ASSUMED STACK GAS MOISTURE, PCT VOL

IS) PERCENT 02
It) PER CENT CO
17) PER CENT 112
18) PER CENT EXCESS AIR
1Q)'MOLECULAR WEIGHT OF STACK GAS, DRY
2Q)MOLECULAR WEIGHT OF STACK GAS, STK CO
2DSTACK GAS SPECIFIC GRAVITY
22)AVG SQUARE ROOT (VEL HEAD), IN H20
23) AVb'R AGE STACK GAS TEMPERATURE, DEG F
2^)AVG SQUARE ROOT (STK TL'!!P*VEL HEAD)
2S)PITOT CORRECTION FACTOR
2&)STACK PRESSURE, IN HG , ABSOLUT'S
27 )S TACK GAS VEL, STACK COiJD, F.P.I',.
2B)STACK AREA, SQ FEET . .
2 . .5
j TJ7T3TI3 	 4—0717^11 	 4 — Cr.-t7TT2-B 	 '
4~'07UU3" i~TT7D'rTrrr i 0~.~mT?T3
JL ~ «-.— ^ 	 L « 	 ^^_^ -J. -~.~~~~~. 	
i T7.uTJ7TT i u.rrrrrrr i ^r.^nr^r ~
4~tJ7t)tT7(T 	 r~u7n>rrrrr 	 r — rr.~rnr2T —
. i 	 • 	 	 	 [ 	 -i 	 _1 	 ,_* 	
| '2.1457 i 0.9553 l H.T^^
1 t.T457 1 0.9553 1 1.786'^_
1_-1A3JL^ 	 L. JL43JO-.. 	 L_...1.43.CL 	
H3)FLUORIDE - WATER SOL . , Ib/hr/ton P205stored 1_.°- P.O.I5. 	 1_ 0',lQfi9Z 	 1__O.OQ12 	 ,
i\H)FLUORIDE - TOTAL, Ib/hr/ton P205 stored "
1 0.0015 1 O.OJ3JDZ 1 0,00_L2_ 	
***5.i7.2J.<">/7/1'y,  70 DEGREES F,  29.92 IHCUES MERCURY***

-------
     TEST NO  -                      '       NO  OF RUNS  -
     PLANT -  BORDEN CHEMICAL    PINEY POINT,  FLA.
     SOURCE -  scrubber Outlet
     TYPE OF  PLANT -  FERTILIZER STORAGE
     CONTROL  EQUIPMENT  -
     POLLUTANTS  SAMPLED  -  FLUORIDES
 I )RUii NUMBER                                 1	J-	1	?	1	3	1
 2) DATE                                       l-Jj^L/JL2--!
 3)TIXE BEGAU                                 1_J_2J_L°_	1
 *t)TIUE EKD                                   l.J-JjJUL	1
 S)BAXO:-!STRIC  PRESSURE,  1/7 JIG             '  L._30	J.__o
 6)METER ORIFICE PRESSURE DROP,  IH HG      i^JlfJJL	-1
 7) VOL DRY CAS,  METER  COND, CUBIC FEET     1__8J_«J-	1
 B) AVER AGE GAS METER TEMPERATURE, DEG F   1_J._OJL_P	i_J_2J.-J	1	121*1	1
 9) VOL DRY GAS,  S.T.P.  ,  CUBIC  FEET        1_JU_._3	JLjJX. 4.3.2	1	£2jLHHl	1
10) TOTAL i!20 COLLECTED,  ML                  JL3Jj3	1_^D-J	1	22	1
11) VOL H20 VAPOR COLLECTED, S.T.P. , CU FTi_l_,3£>	l—l—DI	i__li25.	1
12)STACK GAS MOISTURE,  PERCENT  VOLUME      1_JL'_3	J...2-.3	1	2^2	1
13)ASSUi:SD STACK GAS MOISTURE,  PCT VOL     I__?_j3	1-.2-.4.	l__2.s.it	1
IDPERCEUT C02                               1 ;--	{_-_--	l_.z==.	1
IS)PERCENT 02                                 L.IL1	I--"	!_«=.	1
16)PERCEuT CO              .                   1_I11	1-"--	!_-_-	1'
17)PERCENT 112                                 JLlL"	l-"~	l--~-	ll
1B1PLRCEUT EXCESS AIR                        1__?	J._0	1	2	11
19)MOLECULAR WEIGHT OF  STACK GAS, DRY      L.JrjL.&J?	l.^S^SG	J.	28_^.§.L	1!
20)MOLECULAR WEIGHT OF  STACK GAS, STK CO/7DJL.2?.. 6	1.28^6	J.	2n._Rl_	_[|
21)5TACK GAS SPECIFIC  GRAVITY               1_^J^	l_0j.22	i__9.^2.0.	I1
22)AVG SQUARE  ROOT (VEL HEAD),  IN 1120      1_^J1^	JL 0^.859	J.	2.^11	II
23)AVL'RAGE STACK GAS TEMPERATURE, DEG F   l_.Zlli7	1_V5	1	7.1^2.	I1
24)/iV(/' SQUARE  ROOT (STK TEUPxVEL HEAD)     1_22^21	1_!9.-.8Z8	1	^LV.!	1\
2S)PITOT CORRECTION FACTOR                  1_^8^	1_0A83	1	2.L.11	i1
26)STACK PRESSURE, III  UG , ABSOLUTE   .      i_^°	1_30	_[	30_	jj
27)STAJK GAS VEL, STACK COKD, F.P.M.       l_2504j,5	l_288n._7	J,	^'1^^	jl
2B)ST
-------
SCRUBBER EFFICIENCY

-------
                                           BORDEN CHEMICAL, INC.
                                               GTSP STORAGE
                      Pond Water
             —©-
                       Tail  Gas
                          Scrubber
                                                                         To Pond
RUN
Flow: 83457 (DSCFM)
Fluoride:   2.15 #/hr
Efficiency:  71.6%
Flow:      64844 (DSCFM)
Fluoride:  0.61  (#/hr)
RUN n
            79621
             0.96
             54.2%
           64401
            0.44
RUN #3
            74427
             1.79
             71.5%
           65744
            0.51

-------
APPENDIX B



FIELD DATA

-------
PRELIMINARY MOISTURE DETERMINATION

-------
                          PRELIMINARY MOISTURE CHECK
PLANT   Borden  Chemicals
STACK   Scrubber  Inlet
R\TE    January  24. 1972
   - SAMPLE TIME
METHOD 1
     Dry Bulb Temp.  115°F,      Wet Bulb Temp.   91 °F,     Dew Point Temp.  33 °F.
     Vapor Pressure of H20 @ DP  0.1878  "Hg.          Stack Pressure   29.75  "Hg.
     Moisture Fraction   0.0068 ,                     Dry Air Fraction  0.993? "Hg.
METHOD 2
     Final Dry Test Meter Reading
     Initial Dry Test Meter Reading
     Dry Test Meter Volume Sampled_
     Average Meter Temp_	
     Average Orifice AH
"H20
     Barometric Pressure 9 Orifice Meter
     Dry Gas Volume Sampled @ STP	
     Volume of Condensate
  ml
     Water Vapor Volume 3 STP_
     Moisture Fraction
            Ft
                _"Hg
             Dry Air Fraction

-------
                          PRELIMINARY MOISIUIH: CHECK
PLANT   Borden  Chemicals '
STACK   Storage Outlet
DATE    January 24,  1972
    SAMPLE TIME
METHOD 1
     Dry Bulb Temp.   74°F,      Wet Bulb Temp.   74 °F,     Dew Point Temp.	^°F,
     Vapor Pressure of H20 @ DP  0.8462  "Hg.          Stack Pressure     30    "Hg.
     Moisture Fraction   0.0282 ,                     Dry Air Fraction  0.9718  "Hg.
METHOD 2
     Final Dry Test Meter Reading
     Initial Dry Test Meter Reading
     Dry Test Meter Volume Sampled__
     Average Meter Temp_	
     Average Orifice AH
"H20
     Barometric Pressure 3 Orifice Meter
     Dry Gas Volume Sampled @ STP	
     Volume of Condensate
  ml
          Ft"
            Ft'
                 "Hg
     Water Vapor Volume 3 STP_
     Moisture Fraction
      Ft*
             Dry Air Fraction

-------
FLUORIDE EMISSIONS

-------
/»
SOURCE SAMPLING HELD DATA SHEET •*£" I
Plant ~£%Q rq^^t- ' ^ Mat'l Processing Rate
Sampling Location (ji^H ~ Sc*uM>fr-&t<£"
Date 1/2^1 j2~ Run No. /
Time Start /2/"C~ Time End /JV 3_T •
Sampling Time/Point ytX (£?' /'ji? /t>>W
DB $5" °F, WB — °F, VF @ DP "Hg
Moisture/ %,FDA ,Gas Density Factor
Barometric Press3 ^ "Hg, Stack Press^tf^
Weather f-G-t /*"*
Temp. °F, W/D , W/S
Sample Box No. Meter Box No,
Meter AH@ l'£° Pitot Corr. Factor O.g.,5
Nozzle Dia,O'2/in., Probe Length 8 ft
Probe Heater Setting • ':
Stack Dimensions: Inside Diameter &£> in
Inside Area ft2
Height ft

Sketch of^S
-^
^M
i
. i
\ 1
tatk
\.jj
NN^*' \^^V
O
	 	 —

/7»-
Final Gas Meter Reading (0(0 ~7 . 5" ft3
Initial Gas Meter Reading $~7Q * 5 2 7 ft3
Total Condensate in Impingers
Moisture in Silica Gel "3> „
je- 1*^"
J5* ml/
3 gm^
Silica Gel Container No.£o3 Filter No .7.20 f/
Or sat: C00 •
0,
CO
No
Excess
Air





Test Conducted By: •^T"o /{^ 0_Lf,~HsL
/'
~7~~/3 /r> 7^i ^ /rfe r —

Remarks: ^/a^ V&^c/'A
e//j €. T^ tsfoi^nfr in //^ e.
/ / . • /j . /•
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                                                                                                                          3.:
Port and
Traverse
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1&
/


2~


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Distance
from End
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' (in)
*
?%

iS/
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>
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(ft3)
5^// /f 0
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Head
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%*
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Orifi
Press
rilTT
	 	 1 H2
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/o,o
/Ao

3-V
3-6

Stack Gas
Temp.
(°F)
*r
^r

s^
* £

*£
**

Gas Sample
Temp.@ Dry
Gas Meter
f°F
In
$*

-------
Port land
Traverse
Point No.
I/.


f

•
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' - •
• ,
7


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Distance
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(in)
3/^y


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-------
                                               _.7iRC.._JfTAL _TGIN_.JNG,  «.t,
                                                     Gainesville, Florida
                                              SOURCE SAMPLING  FIELD DATA SHEET
V
   Plant
             son
                   /v.
Sampling Location UJ> /£
Date
^ 7*7 2-
Run No.
Time Start  / 55T
Sampling Time/Point
DB	°F, WB	'
Moisture^/	I, FDA
Barometric Press 3°
Weather   (^,/f»^^
Temp.	°F, W/D
                                 2.
                         Time End   /JT.' ff
                       F, VF  8 DP
                     'Hg
                       	,Gas Density F act or_
                       'Hg, Stack PresS'f
                              ,W/S
  Meter 'Box No.
   Sample Box No, _
   Meter AH@/»lg Pitot  Corr. Factor   O.?3
   Nozzle Dia.jg,jL^in. ,  Probe Length
   Probe Heater Setting _
                      ft
   Stack Dimensions:  Inside  Diameter
                     Inside  Area  .
                     Height	
                      in
                    Tt2
                    " ft

                                           /
                                                                           Mat'l Processing Rate	
                                                                           Final Gas Meter Reading	
                                                                           Initial Gas Meter Reading
                                                                           Total Condensate in Impingers
                                                                           Moisture in Silica Gel       ~z
                                                                                                              ml
                                                                                                                          gm
                                                                           Silica Gel Container No.
                                                                           Orsat:  C07
                                                                                     LJ  i •-•—..
                                                                                   02 _____
                                                                                   CO
                                                                                                  Filter No.
                                                                       Excess
                                                                         Air
                                                       Test Conducted by:_
                                                                  Remarks:
Port and
Traverse
Point No.
/

?~

3-


Distance
from End
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(in.)
*3&
./
<^6
/
/*'2fc


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Time
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141°
/¥/-**
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(ft3)
617S5°
&$<{,<$
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700,~2f
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7/7-7
/
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(°F)
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^7
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-------
Port and
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4
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(ft3)
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?2 £' ^
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-------
Y
   Plant
cL
                                               I  . JfcQN _. -lAL _ .'JNEL. „ t,
                                                    Gainesville,  Florida
                                              SOURCE SAMPLING FIELD DATA SHEET
Sampling Location Id, H , Sc ru^fier* 3* /<•/
Date /-l^t- -7 ^ Run No. $
Time Start /C'rCT Time End /"/V/C?
Sampling Time/Point /O y^r^( /?o, ToT*-l
DB °F, WB °F, VF @ DP ' "Hg^
Moisture I* I, FDA , Gas Density Fact or
Barometric Press^6"Hg, Stack Press2If,Zjr"Hg
Weather
Temp. °F, W/D ,W/S
Sample Box No. Meter Box No.
Meter AH@ /.£# Pitot Corr. Factor ,$%
Nozzle Dia. ,ZfTin. , Probe Length ft
Probe Heater Setting O ^
Stack Dimensions: Inside Diameter ££ in^fc
Inside Area . ft^
Height ft



)












Mat'l Processing Rate	
Final Gas Meter Reading	
Initial Gas Meter Reading77^,
                                                                                                  ft3
                                                                             Total  Condensate  in  Impingers
                                                                             Moisture  in Silica Gel
                                                                                                 ml
                                                                             Silica Gel  Container No. ?
s;i
f 3.>tf
3.Sf

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Temp.
(°F)
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Temp.S Dry
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-------
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Plant  J?pjfD£A/
                                                           IGIN_,JNG,  ^fc,
                                                 Gainesville,  Florida
                                           SOURCE SAMPLING FIELD DATA SHEET
Sampling Location STotffi££ T>M/*
Date  /-2*/-72-    Run No.       /
                                          /5/A/A FLA
Time Start /2.' 2O	Time End
Sampling Time/Point 2./, /g^

MoistureZ 7*%, FDA 97' £? Gas Density Factor
Barometric Press ^Tcl'Hg. Stack Press
Weather
           L°F>  W/D    —   ,W/S  ""
Sample Box No,    /    Meter Box No.
Meter AH@ /»7^itot Corr. Factor  i
                                      /
Nozzle Dia._/Vin.,  Probe Length
           1 ^ •'" t "'           _     —
Probe Heater Setting_	^ o%
Stack Dimensions:  Inside Diameter
                  Inside Area__.
                  Height	~
Mat'l Processing Rate
                                                                         Final Gas Meter Reading   /S?' 3-S "7    ft3
                                                                         Initial Gas Meter Reading  ~?2.,/3~7
                                                                         Total Condensate in Impingers
                                                                         Moisture in Silica Gel
                                                                         Silica Gel Container
                                                                         Orsat:
        C02_
        °2 _
        CO _
        N2 _
     Excess
       Air
                                                                          Test  Conducted by:     /?>?//».<:. A-
                                                                          Remarks :
                                                                                         L o /}
                                         ft
                            Vr7o X £•/»/" .<"
Port and
Traverse
Point No.
O •+£> \
j&u.** '
pnnvifl **~ I
( 2
3
^- v
5"
£
7
Distance
from End
of Port
(in.)
J" •
3
s
7
Cf
11
13
Clock
Time
«^
~-
—
/Z!Z^
/^2-',2S
/2.132-
7:2. ',3&
Gas Meter
Reading
Cft3)
, —
—
— .
"7StH-
7~7.*f
^/,i-
?s5",5
Stack
Velocity
Head
("H20)
. 	 •
-—
	 r.
o./d
,€D« X&
<0i 7^
^^f^
Meter
Orifice
Press. Diff.
C'H20)
Calc.
>-
l\n
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,1/2,
l,.o£
3,, 20
3.^
Actual
—
E^-flr/i
— _
.¥2-
l*o£
3,2.0
3.^
Stack Gas
Temp.
^~
/f |/£-^,
	 ^ '
~7^
75"
75-
IS'
Gas Sample
Temp.@ Dry
Gas Meter
C°F)
In
Out

VI
—
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.^u
^2^
	
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rif ?
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Sample
Box
Temp.
C°F)
^—
—
— .
— .
—
—
-r-
Last
Mpirger
Test
«?rr~
««— .
	 	
77
75-
7^"
7^
Vacuuir;
on I
Samplej
Train
("Hg)
'--*
. 	 .
• — •
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-------
Port  and
Traverse
Point No.
Distance
from End
of Port
  (in)
                  Clock
                  Time
Gas Meter
Reading
 (ft3)
Stack
Velocity
Head
C"H20)
          Meter
          Orifice
          Press. Diff.
            ("H20)
                                                       Calc.   Actual
Stack Gas
  Temp.
Gas Sample
Temp. @ Dry
Gas Meter
  ra-
                                                                                   Out
Sample
 Box
 Temp.
Last
Impinger
Temp.
 ra
Vacuum
  on  *1
Sample j
Train
               17
       in
                                                                                             /  'v-
                                                                                             e?' o
       II
       /Z
       73
JLt
  2;
  23
  2S
              27
                           /o7-
JSLIJ..
                       3.7(9
                                                                  7V
                                                                                            "75
                                                     7,5"

                                                                                      75
                                                                          7',?
                                                                         _Zi£.
      n
              31
              37
           /3:/2
                                                                  J2£
                                                                   7
                                  33'
                                                  3.y<
                                                            7

                           /375"
                                                                .
                                                            7S
                                                                                                  7?
                                                                  77
                                                                                              7; *
                                                             7
      zo
           )3>'2g
                                                                                            2*L
      Z/
            13^2-
                                                                         /37
      2.2-
                     /o.
                                         o.
                       3-,
                            7.5"
                                                      77
      2.3
                                           5-55
                                                         3.35
                                              /37
      1*4
                                                                 /33_
                                                                                   V,
                                                                                    .r

-------
Plant
                                fifLL
                                               GROJ   HAL    BIN!	."KG,  _..
                                                  Gainesville,  Florida
                                            SOURCE SAMPLING  FIELD DATA SHEET
                                     FV
Sampling Location^;
Date  A- 2 '<°lf, W/D_
Sample Box No.   I
Meter AHg /-?2,Pitot Corr.
Nozzle Dia. fy  in., Probe
Probe Heater Setting	
                      Meter Box No.
Stack Dimensions: Inside Diameter
                  Inside Area
                  Height
                                                                          Mat'l  Processing Rate
                                                                          Final  Gas Meter Reading
                                                                          Initial  Gas Meter Reading
                                                                           Total  Condensate in Impingers
                                                                           Moisture in Silica Gel
Silica Gel Container No
Orsat:  C02	
. ^PT>1
                                                                                                          Filter
                           ,W/S
                                                                                   02 _
                                                                                   CO _
                                                                                   N2 _
                                                                                Excess
                                                                                  Air
                                                                           Test Conducted by:
                                                                                                  &-
                                                                                                    /?.
                                                                           Remarks:
' HECTfyfiJf. u L*fL