72-MM-23
                             (REPORT NUMBER]
AIR POLLUTION  EMISSION  TES
                BLECKLEY FARM SERVICE COMPANY
                           (PLANT NAME)
                         (COTTON GIN)
                      COCHRAN, GEORGIA
                         (PLANT ADDRESS)
          U. S. ENVIRONMENTAL PROTECTION AGENCY
               Office of Air and Water Programs
           Office of Air Quality Planning and Standards
           Emission Standards and Engineering Division
                Emission Measurement Branch
              Research Triangle Park, N. C.  27711

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      PARTICULATE EMISSION MEASUREMENTS

              FROM COTTON GINS
                Plant Tested

        Bleckley Farm Service Company
              Cochran, Georgia

                November  19 7^

       EMB Project Report No. 72-MM-23
                Prepared for

      Environmental Protection Agency
Office of Air Quality Planning and Standards
       Emission Measurement Branch
         Research Triangle Park   :
          North Carolina 27711
                    by
              W.  R.  Feairheller
               D.  L.  Harris
        Monsanto Research Corporation
              Dayton Laboratory
              1515 Nicholas Road
              Dayton, Ohio  45^07
      Report Reviewed by John W. Snyder
     Contract No. 68-02-0226, Task No. 6

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                       TABLE OF CONTENTS
  I.   INTRODUCTION                                        1
 II.   SUMMARY AND DISCUSSION OF RESULTS                   6
III.   PROCESS DESCRIPTION AND OPERATION                  26
 IV.   SAMPLING AND ANALYTICAL PROCEDURES                 34
      A.  LOCATION OF SAMPLING POINTS                    34
      B.  SAMPLING PROCEDURES     .                       39
      C.  ANALYTICAL PROCEDURES                          45

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                      LIST OF TABLES
 1.    Summary of Emission Measurements                     9

 2.    Sampling Schedule                  '                12
                                         i
 3.    Efficiency Comparison Results                       13

 4.    Summary of Results - Inlet to  Unloading Separator
                           Cyclones  - Point  13           15

 5.    Summary of Results - Outlet of Unloading Separator
                           Cyclones  - Point  1            16

 6.    Summary of Results - Outlet of Unloading Separator
                           Cyclones  - Point  18           17
 7.    Summary of Results - Inlet to  Inclined Cleaner
                           Cyclones  - Point  10           18

 8.    Summary of Results - Outlet of Inclined Cleaner
                           Cyclones  - Point  4            19

 9.    Summary of Results - Inlet to  Extracter Feeder,
                           Gin Stand Cyclones - Point 8  20

10.    Summary of Results - Outlet of Extracter Feeder,
                           Gin Stand Cyclones - Point 6  21

11.    Summary of Results - Inlet to  Battery  Condenser
                           Filter -  Point 16             22

12.    Summary of Results - Outlet of Battery Condenser
                           Filter -  Point 17             23

13.    Summary of Results - Outlet of Trash Hopper
                           Cyclone - Point 7             24

14.    Summary of Results - EPA-5 and High Volume Samplers
                           Comparison - Point 18         25
                            ii

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                      LIST OF FIGURES
1.   Schematic Diagram of Control Devices,  Bleckley  Farm
     Service Company, Cochran,  Georgia                       3
2.   Plant Flow Diagram                                     27
3.   Location of Emission Control Devices                    28
4.   Schematic of In-Line Filter Showing Ducts  and
     Sampling Ports                                         36
5.   Diagram of Straightening Vane Construction             38
6.   Schematic Diagram of Outlet Ducts,  1,  18,  1A, 18A,  and
     Inlet Duct 13                       ,                   40
7.   Schematic Diagram of Outlet Ducts 4 and 4A,  and Inlet
     Duct 10                                                *»1
8    Schematic Diagram of Inlet Duct 8,  and Outlet Ducts
     6 and 6A                                               42
                             ill

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                       SECTION I
                     INTRODUCTION

This test is part of the Cotton Ginning Industry Study, a
project of the Industrial Survey Section, Industrial Studies
Branch, Emission Standards and Engineering Division, Office
of Air Quality Planning and Standards, Environmental Pro-
tection Agency.  The field test work was directed by Joseph
Bazes, Field Testing Section, Emission Measurement Branch.
The sampling was performed by Monsanto Research Corporation.
The cotton Ginning Industry Study is being conducted by
William 0. Herring, Industrial Survey Section.

Under the Clean Air Act of 1970, the Environmental Protection
Agency is given the responsibility of establishing performance
standards for new installations or modifications to existing
installations in stationary source categories.  As a con-
tractor, Monsanto Research Corporation, under the Environ-
mental Protection Agency's "Field Sampling of Atmospheric
Emissions" Program, was asked to provide emission data from
the Bleckley Farm Service Company, Cochran, Georgia.  The
cotton gins selected and studied were equipped with the
best types of pollution control equipment currently availa-
ble.

This report tabulates the data collected at the Bleckley
Farm Service Company during the period from October 9 to
October 20, 1972.  In this cotton gin, vacuum is used to
remove the field picked cotton from the cotton wagons and

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then the material  inside the gin is moved  from one operation
to the next by  a moving air system.  Air moves the material
to the ginning  machines for removal of dirt,  plant material,
the cotton seeds,  and fine lint, and finally  to the battery
condenser and the  press or baling machine.  The air from
the unloader, feeder, dryer, and lint cleaners is  exhausted
from the building  into a group of fourteen cyclones, while
the air from the lint cleaner condenser and battery condenser
is exhausted through rotary screen in-line filters.  The
trash, including plant debris and dirt, is directed to a
cyclone mounted on a trash hopper.  A schematic diagram of
the control devices with respect to the building and indi-
cating which of the devices were sampled is shown in Figure 1
The description of the device and the designation of the
sample point numbers are as. follows:
                                    Sample Point Nurabe r s
Exhaust from:
Battery
Condenser
Lint Cleaner
Condenser*
Unloading
Separator
Inclined
Cleaner
Extractor
Feeders, Gin
Stands, Unit-
air Lint
Cleaners
Inlet to Outlet from
Control Device Control Device Control Devicp
In-line filter 16 17, 17A
In-Line filter 15 It, l^A
Cyclone (4) 13 1, 1A, 18, 18A
Cyclone (2) 10 1), 1)A
Cyclone (2) 8 6, 6A
         Previous
         Cyclones and
         In-line Filters
         (Trash)      Cyclone (1)         -     7
             * No flow was detected on the outlet of this
               device. No samples were collected.

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BATTERY
CONDENSER
LINT CLEANER
CONDENSER
UNLOADING
SEPARATOR
INCLINED
CLEANER
EXTRACTOR
FEEDERS GIN STANDS
UNIT AIR
LINT CLEANERS
                                    ©-O
 Figure 1.  Schematic Diagram of Control Devices, Bleckley
            Farm Services  Co.,  Cochran, Georgia
             (Note:   No flow  was detected on  outlets 14 and
              14A, therefore  no samples were  collected)

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The major emphasis of the study was to obtain accurate data
on the particulate emissions and the efficiency of the con-
trol device for the removal of particulate matter.  To
accomplish this objective, simultaneous measurements were
made on the inlets and atmospheric outlets of the devices.
Outlets to the atmosphere were measured for particulate
concentrations using Method 5» "Determination of Particulate
Emissions from Stationary Sources."  Other procedures that
were required during the study included Method 1, "Sample
and Velocity Traverses for Stationary Sources," Method 2,
Determination of Stack Gas Velocity and Volumetric Plow
Rate (Type S Pitot Tube)," Method 3, "Gas Analysis for
Carbon Dioxide, Excess Air and Dry Molecular Weight," and
Method 4, "Determination of Moisture in Stack Gases."  The
particulate loading in the inlets to the control devices
was  determined using a high-volume source sampler con-
structed by the EPA and operated by both EPA and MRC personnel
A detailed description of this sampler.is given in a later
section of this report.  Pesticide analysis was performed on
samples of seed cotton and gin trash.  Samples of particu-
late collected on runs 18-1, and 2 were analyzed for trace
metal and from runs  18-3, and 4 for arsenic content.

Extensive modifications were required to prepare the cotton
gin for sampling.  The outlets of the in-line filters, partly
covered with a rain shield, were vented directly in the out-
side air.  This shield was removed and replaced on both sides
with a 42" diameter duct 160" long.  The cyclone outlets were
also covered with a rain shield.  As the gas flow from the
cyclone would definitely have a cyclonic flow pattern, the
rain shields were removed and replaced with a large radius
180° bend, 16" I.D., to direct the flow downward followed by
a straightening vane to eliminate cyclonic' flow, then a
straight duct 16" in diameter by 194" long.  The entire duct

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modification for the cyclones resembled a large "candy cane."
The reasons for this type of duct system were to:  (1) pro-
vide a long straight run that would be close to the ground,
(2) to permit incorporation of the straightening vane to
eliminate cyclonic flow, and (3) provide sufficient duct
after the vane to provide relatively stable flow at the sam-
pling point.  Detail of these modifications are given in
Section IV.

The following.sections of this report include (1) summary
of results, (2) description of the process, (3) location of
sampling points and traverse data, (^) process operating
conditions, and (5) sampling and analytical procedures.
Appendix C includes all field data from this cotton gin.

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                      SECTION II
          SUMMARY AND DISCUSSION OP RESULTS


The Bleckley Farm Service Company cotton gin employs both
in-line filters and cyclones as control devices.   The in-
line filters, used on emissions from the battery  condenser
and the lint cleaner condenser, have a single inlet pipe
leading to the rotating screen filter.  Each filter has two
outlets venting directly from the side of the filter into
the outside air.  A small rain shield was used to cover the
outlet.  Sampling criteria required that the rain shields
be removed and replaced with long horizontal ducts.

The exhaust from the other systems (unloading separator,
inclined cleaner, extractor feeders, gin stands,  and trash
lines) were directed to cyclones, which were grouped in
banks of 2 or 4 from each inlet line.  The cyclones were
capped with a rain shield, adjusted by the gin builder to
yield a back pressure that would provide good separation
efficiency.  Such a system however, is not suitable for
testing from two points of view.  First, no suitable loca-
tion is available in the exhaust from the cyclone, due to
the short length of outlet pipe, and second, the  flow from
these devices is cyclonic and thus would require  a device to
eliminate the spiral flow pattern.  The sampling  modifica-
tions for these devices were required to provide  a sampling
location consistent with good sampling practice and also
include straightening vanes.

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Specific details of the duct additions are given in Section
III A.  In brief, the in-line filters were provided with
two long ducts attached to each outlet.  The cyclones were
provided with a large radius 180° bends, a straighten vane
and a long straight length of pipe in place of the rain
shield.  The duct additions resembled a large "candy cane."
Each cyclone in a bank was provided with the same type of
device so that charges in back pressure would not change the
proportion of air to each cyclone in the bank.

Measurements of the static pressure were made on the inlet
to each bank of cyclones before the rain sheilds were re-
moved.  After installation of the candy canes the measure-
ments were repeated.  The static pressure data referring to
the sample point number indicated in the Introduction, are
as follows:
                  Static Pressure     Static Pressure
     Inlet to      with Rain Cap      with Candy Cane
     Point No.   (inches of water)   (inches of water)
         7              5.0                 6.5
         8           0.5 to  1.0          .  0.85
        10          not available           2.0
        13          -0.3 to -1.0            0.1

This data indicates that the candy cane duct design does
increase the static pressure in the system and may change
the operation of the cyclone.  Without actual velocity data
on the inlet, we must assume that an increase in static
pressure means a decrease in velocity in the duct.  This
would mean that the cyclone would not be as efficient and,
therefore, the emission rate with the candy cane would be
higher.  If, however, the fan on the system is able to main-
tain the velocity under the increased static pressure, then
the emission rate would not be appreciably different under
the two conditions.

                          . 7

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Although the outlet of the cyclones varied from 16" to 17",
a 16" diameter "candy cane" was used for all units.  An
adapter was constructed for the outlets that were over 16"
to allow the 16" duct to fit.  All joints were sealed with
furnace tape.

A summary of the emission data collected at this gin is given
in Table I.  The test numbers indicate both the sampling
point (as shown in the Introduction) as well as the run num-
ber at that point.

Inlets to each control device could not be sampled by the
EPA 5 Particulate technique due to the large size of the
material in the duct.  A high volume in-stack sampler, de-
signed and fabricated by EPA was employed at these points.
This device is described in detail in Section IV and
Appendix F.  A comparison study of the high volume and the
EPA 5 sampling trains was made on duct 18, run numbers 18-4
and 18-4H.  For comparison, only the front half mass data
(from probe tip to filter) from run 18-4 can be compared to
the high volume data.  The emission rate in Ib/hr was found
to be 0.597 for the EPA 5 Method and 1.32 for the high vol-
ume method.  The high volume run was above acceptable iso-
kinetic conditions (111%), but this is not high enough to
account for the difference in the observed emission rates.
One possible reason for this difference is that the high
volume sampler could collect large particles that could not
pass through the EPA 5 probe tip.  If this were the case,
these particles would tend to clog the probe tip of the
EPA 5 sampling train.  This did not occur during the run.

Sample Number 18-4 (by EPA 5) was also used for arsenic
analysis.  The second impinger in the sampling train was
filled with 2% NaOH instead of water.  The solution was
then analyzed by EPA for arsenic content.  The filter and

                           8

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                        Table 1
            SUMMARY OF EMISSION MEASUREMENTS
MADE AT BLECKLY FARM SERVICES COMPANY. COCHRAN,
                                                                                     GEORGIA
Date
1972
10/10
10/10
10/10
10/10
10/11
10/11
10/11
10/12
10/12
10/13
10/16
10/16
10/16
10/16
10/16
10/16
10/16
10/16
10/17
10/17
10/18
10/18
10/18
10/18
10/18
10/18
10/19
10/19
10/19
10/19
10/19
Test
No.
16-1
16-2
17-1
17-2
7-1
16-3
17-3
6-1
7-2
8-2
4-1
4-2
6-2
6-3
8-3
8-4
10-1
10-2
4-3
10-3
1-1
1-2
13-1
13-2
18-1
18-2
1-3
13-3
18-3
18-4H
18-4
Sampling
Test Site Method
Inlet Battery Condenser High Volume
Inlet Battery Condenser High Volume
Outlet Battery Condenser Method 5
Outlet Battery Condenser Method 5
Trash Hopper Cyclone Method 5
Inlet Battery Condenser High Volume
Outlet Battery Condenser Method 5
Extractor Feeder Cyclone Method 5
Trash Hopper Cyclone Method 5
Inlet/Extractor Feeders High Volume
Inclined Cleaner Cyclone Method 5
Inclined Cleaner Cyclone Method 5
Extractor Feeder Cyclone Method 5
Extractor Feeder Cyclone Method 5
Inlet/Extractor Feeders High Volume
Inlet/Extractor Feeders High Volume
Inlet Inclined Cleaner High Volume
Inlet Inclined Cleaner High Volume
Inclined Cleaner Cyclone Method 5
Inlet Inclined Cleaner High Volume
Unloading Separator Cyc. Method 5
Unloading Separator Cyc. Method 5
Inlet Unloading Separator High Volume
Inlet Unloading Separator High Volume
Unloading Separator Cyc. Method 5
Unloading Separator Cyc. Method 5
Unloading Separator Cyc. Method 5
Inlet Unloading Separator High Volume
Unloading Separator Cyc. Method 5
Unloading Separator Cyc. High Volume
Unloading Separator Cyc. Method 5-As.
Average
Velocity
Average
Temperature
ft/sec (m/sec) °F (°C)
65.2
60.9
12.2
12.4
37.7
59-7
13.0
18.0
36.5
69.0
26.7
28.0
13.8
15.8
70.5
70.4
65.9
61.9
26.8
70.7
18.8
20.0
65-9
79-9
17-7
18.2
18.8
80.4
18.7
18.1
20.3
(19.9 )
(18.6 )
( 3.72)
( 3.77)
(11.5 )
(18.2 )
( 3.96)
( 5.49)
(11.1 )
(21.0 )
( 8.14)
( 8.53)
( 4.20)
( 4.82)
(21.5 )
(21.5 )
(20.1 )
(18.9 )
( 8.19)
(21.6 )
( 5.73)
( 6.10)
(20.1 )
(24.4 )
( 5.39)
( 5.55)
( 5.73)
(24.5 )
( 5-70)
( 5.52)
( 6.19)
88.7
92.5
114.
101.
98.0
87.7
103-
111.
105.
90.0
124.
121.
95.0
96.0
111.
111.
163.
163.
97.0
150.
106.
107.
102.
95.0
109.
96.0
92.0
97.3
98.0
82.0
82.0
(31.5)
(33.6)
(45.6)
(38.3)
(36.7)
(30.9)
(39.4)
(43.9)
(40.6)
(32.2)
(51.1)
(49.4)
(34.0)
(35.6)
(43.9)
(43.9)
(72.8)
(72.8)
(30.1)
(65.6)
(41.1).
(41.7)
(38.9)
(35.0)
(42.8)
(35.6)
(33.3)
(36.3)
(36.7)
(27.8)
(27.8)
% 0,
21.0
21.0
21.0
21.0
21.4
21.0
21.0
21.4
21.4
21.4
21.2
21.2
21.4
21.4
21.4
21.4
21.2
21.2
21.2
21.2
21.4
21.4
21.4
21.4
21.4
21.4
21.4
21.4
21.4
21.4
21.4
jgCO;
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
it CO
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
%N2
79.0
79.0
79.0
79.0
78.6
79.0
79.0
78.6
78.6
78.6
78.8
78.8
78.6
78.6
78.6
78.6
78.8
78.8
78.8
78.8
78.6
78.6
78.6
78.6
78.6
78.6
78.6
78.6
78.6
78.6
78.6
Particulate
Emission Rate*
Ibs/hr
8.61
8.44
2.57
3.44
1.13
11.0
2.71
0.532
1.32
174.0
0.838
0.591
0.272
0.220
145.0
205.0
43.3
59.7
0.564
38.5
0.709
0.855
40.3
21.3
1.04
1.09
0.748
34.1
0.785
1.32
0.597
_ (kg/hr) .
(3.9D
(3.83)
(1.17)
(1.56)
(0.513)
(4.99)
(1.23)
(0.241)
(.599)
(78.8)
(0.380)
(.263)
(0.123)
(0.100)
(65.7)
(92.9)
(19.6)
(27.1)
(.256)
(17-5)
(.322)
(.388)
(18.3)
(9.66)
(.472)
(.494)
(.339)
(15.5)
(.356)
(..599)
(.271)
itHgO
2.0
2.0
1.87
0.0
0.72
2.0
0.5
1.66'
1.05
1.64
6.34
4.58
2.42
1.81
2.42
1.80
6.34
4.55
3.02
3.01
1.87
1.45
1.86
1.44
2.60
1.88
1.28
1.28
2.17
0.86
0.87
*For Method 5 Samples, Emission Rate is Total Emission Rate

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dried residues from all parts of the sampling train were also
analyzed for arsenic.  The results indicated (1)  that a
greater portion of the arsenic is caught in the impingers
rather than in the probe and filter, and (2) the  NaOH is not
required to trap the arsenic.  This data, presented in Ap-
pendix I is summarized as follows:

                                    18-3      18-4
       Total Gas Volume DSCF        22.8      26.0
       Arsenic Front Half (mg)       1.15      1-75
       Arsenic Total Train (mg)      7.85      6.60
       Arsenic in Blanks            <0.4      <0.4

Residues from runs 18-1 and 18-2 were analyzed by Batelle
Memorial Institute for trace metal content.  This data is
presented in Appendix J.  The elements Ba, Mg, Si, Ca, K,
Na, Fe, Cu, and As were found in appreciable quantities.

Pesticides analysis was performed on the gin trash and seed
cotton.  High concentrations of both organochlorihe and
organophosphous compounds were found.  The concentrations
levels in the trash is considerably higher than in the seed
cotton.  The data given in detail in Appendix H is summa-
rized as follows:

             Concentrations ppm by Weight
        Compound             Seed Cotton    . Trash
        p,p'-DDT                 4.1         19.5
        o,p-DDT                  0.63         3.57
        Toxaphene                4.6         22.5
        Methyl Parathion         0.22         0.33

Other material found included degradation products of DDT
and also endrin, the latter just barely detectable.

                           10

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It was assumed that the loading in grains/DSCF would be the
same in each portion of the system and the outlet emission
rate in Ib/hr would vary with the velocity at each outlet
point.  Thus, the emission rate of each outlet is known or
calculated and the total emissions is equal to the sum of
the emission from all outlets in the system.  As the inlet
loading is known from the high volume samplings runs, an
efficiency can be calculated in each individual control sys-
tem, either cyclone bank or in-line filter.

The high volume sampler does not collect any material or
condensate after the filter.  The data from the high volume
runs would, therefore, correlate with the "front half" of
the Method 5 samples.  Only "front half" data was used to
determine efficiencies.  The sampling schedule, shown in
Table 2 describes which units were sampled or traversed dur-
ing the same time interval.  Additional information on the
schedule are given in Appendix G - Sampling Log.

The efficiency data on the control devices is summarized in
Table 3.  The complete data and example calculations on all
inlet ducts, sampled and unsampled outlet ducts are given
in Appendix A1-A6.  In general, the efficiencies of the
cyclones varied from at low of 82.9% to 99.9$.  The cyclones
on the unloading separator are the least efficient indica-
ting that the cyclones could not easily separate the  type
of material being fed to them.  The inclined cleaner and
extractor feeder cyclones were much more efficient.  Only
very short sampling runs were possible on the inlets to these
cyclones due to the high loadings and the large size of
debris present in the ducts.

The results on the cyclones indicate they are very effi-
cient in removing large material from fine material, but
                           11

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                               TABLE 2

                          SAMPLING SCHEDULE
                                                        Sample Point No.
Date
10/10
10/10
10/11
10/18
10/18
10/19
10/19
10/16
10/16
10/17
10/12
10/16
10/16
10/16
10/11
10/12
Exhaust Prom
Battery Condenser
Battery Condenser
Battery Condenser
Unloading
Unloading
Unloading
Unloading
Inclined
Inclined
Inclined
Extractor
Extractor
Extractor

Separator
Separator
Separator
Separator
Cleaner
Cleaner
Cleaner
Feeders, etc.
Feeders, etc.
Feeders, etc.

Trash Hopper
Trash Hopper
Control
In-line
In-line
In-line
Cyclone
Cyclone
Cyclone
Cyclone
Cyclone
Cyclone
Cyclone
Cyclone
Cyclone
Cyclone

Cyclone
Cyclone
Device
Filter
Filter
Filter
(4)
(4)
(4)
(4)
(2)
(2)
(2)
(2)
(2)
(2)

U)
'(•1)
Inlet
16-1
16-2
16-3
13-1
13-2
13-3

10-1
10-2
10-3
*
8-2
8-3
8-4
—
—
Outlet
17-1
17-2
17-3
1-1, 18-1
1-2, 18-2
1-3, 18-3
18-4, 18-4H
4-1
4-2
4-3
6-1
6-2
6-3
—
7-1
7-2
Traversed Duct
17A-1
17A-2
17A-3
1A-1,
1A-2,
1A-3,

4A-1
4A-2
4A-3
6A-1
6A-2
6A-3
—
—
—


18A-1
18A-2
18 A- 3










* High Volume samples  run was  aborted.
  clogged the sampler.
The high particulate loading in  duct
                                 12

-------
     Process  and
    Control Device


Unloading Separator
  Cyclone
Inclined Cleaner -
  Cyclone
Extractor Feeder, Gin
  Stands - Cyclone
Battery Condenser -
In-line Filter
                                  TABLE 3

                       EFFICIENCY COMPARISON SUMMARY
Run Numbers
Inlet
13-1
13-2
13-3
Outlet
1-1,
18-1
1-2,
18-2
1-3,
18-3
1A-1,
, 18A-1
1A-2,
, 18A-2
1A-3,
, 18A-3
Average
10-1
10-2
10-3
4-1,
4-2,
4-3,
4A-1,
4 A- 2
4A-3
Average
8-2
8-3
8-4
Averaj
16-1
16-2
16-3
6-1,
6-2,
6-3,
*e .
17-1
17-2
17-3
6A-1
6A-2
6A-3

, 17A-1
, 17A-2
, 17A-3
Average
(Hi-vol)
Inlet
Ib/hr
40.
21.
3^.
31.
43.
59-
38.
47.
174.
145.
205-
175-
8.
8.
11.
9.
3
3
1
9
3
7
5
2
7
9
8
5
64
44
0
36
Outlet
Ib/hr
3
3
2
3
1
0
0
1
1
0
0
0
•4
5
3
4
.10
.65
.34
.03
.331
.918
• 934
.06
.01
.473
.304
.596
.67.
.35
.80
.61 . .
Efficiency
92.3
82
93
90
96
98
97
97
99
99
99
99
45
36
65
50
• 9
.1
.5
.9
.5
.6
.8
.4
• 7
• 9
.7
.9
.6 .
.5 •
.7
                                     13

-------
are not very efficient in separating relatively fine mater-
ial from the gas stream.

As might be expected, the in-line filters are not very effi-
cient.  These filters consist of a rotating screen of wire
mesh and as a result, can not remove any fine particles from
the gas stream.  The separation efficiency will increase as
the screen becomes clogged, but when this happens, the ve-
locity from the filter outlets will be greatly decreased.

A summary of the data collected on each individual sampling
site is given in Tables 4-14.  In these tables the data in
parenthesis is the value given in metric units.  Also in-
cluded in these tables are the values of the loading in terms
of Ibs of cotton produced.  This value allows the emission
rate to vary with the production which is more representa-
tive than the grains/DSCP or Ibs/hr emission figures.

-------
                                  Table  4  -  SUMMARY  OF RESULTS - INLET TO UNLOADING SEPARATOR CYCLONE - POINT 13
Ul
       Run  Number:

       Date:

       Method Type:
       Volume of gas  sampled-DSCFMNm3)"
       Percent Moisture by Volume
       Average Stack  Temperature-°P-(°C)
       Stack  Volumetric Flow Rate-DSCFM2-(Nm3/sec)
       Stack  Volumetric Plow Rate-ACFM3-(m3/sec)
       Percent Isokinetic
       Product Rate-ton lint cotton/hr-(M ton/hr)5
       Duration of run - minutes

       Particulates - probe, cyclone
                      and filter catch
       mg
       grains/DSCF6-(mg/Nm3)
       lb/hr-(kg/hr)
       Ib/ton of lint cotton produced
       (Kg/M  ton of lint cotton produced)
                                                                  13-1
    10-18-72
High Vol. Sampler

  2795  (79.2)
      1.86
   102  (38.9)
  4535  (2.14)
  4849  (2.29)
       106
  1.98  (1.80)
       64.0
     188356.4
1040  (2.38xl06)
40.3  (18.3)
20.4  (10.2)
                           13-2
    10-18-72
High Vol. Sampler

  3110  (88.1)
    95
  5570
  5878

  2.04
 .44
  (35)
  (2.63)
  (2.77)
  97
  (1.85)
 64.0
 446
21.3
10.4
89903.8
(1.02X106)
(9.66)
(5.22)
13-3
10-19-72
High Vol. Sampler
3267 (92.5)
1.28
97.2 (36.2)
5622 (2.65
5914 (2.79)
101
2.96 (2.69)
64.0
150071.7
709 (1.62xl06)
34.1 (15.5)
11.5 (5.76)
Average


3057 (86.6)
1.53
97-3 (36-3)
5243 (2.47)
5547 (2.62)
101
2.33 (2.11)
64.0
142777.3
732 (1.68xl06)
31.9 (14.5)
14 ..1 (7.06)
       !Dry Standard Cubic Feet @ 70°F, 29.92 in Hg
       2Dry Standard Cubic Feet per Minute @70°F, 29-92 in Hg
       3Actual Cubic Feed per Minute - Stack Conditions
       '•Normal Cubic Meters at 21.1°C, 760 mm Hg
       5Metric Tons per Hour (1 metric ton = 1000 Kg)
       6Grains per Dry Standard Cubic Feet

-------
                           Table 5 - SUMMARY OF RESULTS - OUTLET OF UNLOADING SEPARATOR CYCLONES  -  POINT  1
Run Number:

Date:

Method Type:

Volume of gas sampled-DSCF^CNm3)1*
Percent Moisture by Volume
Average Stack Temperature-°F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(NmVsec)
Stack Volumetric Flow Rate-ACFM3-(m3/sec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes

Particulates - probe, cyclone
               and filter catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(kg/M ton of lint cotton produced)

Particulates - total catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
percent impinger catch
                                                              1-1
                                                                                   1-2
   10-18-72

  EPA Method 5

23.12  (0.657)
     1.87
  106  (11.1)
 1460  (0.689)
 1570 . (0.74D
    105.6
 1.98  (1.80)
      64.0
     72.8
 0.0483  (111)
 0.604  (0.274)
  .305  (.152)
     85.4
 0.0567  (130)
 0.709  (0.322)
  .358  (.179)
                                                                                                        1-3
  10-18-72
 EPA Method 5
24.8  (0.702)
    1.45
 107  (41.7)
1550  (0.732)
1670  (0.788)
   107.3
2.04  (1.85)'
     64.0
    92.2
0.0573  (131)
0.761  (0.345)
 .373  (.186)
   103.7
0.0644  (147)
0.855  (0.388)
 .419  (.210)

    11.1
  10-19-72

 EPA Method 5

24.2  (0.685)
    1.28
  92  (33.3)
1510  (0.713)
1580  (0.746)
   107.2
2.96  (2.69)
     64.0
    73.0
0.0465  (106)
0.602  (0.273)
 .203  (.101)
    90.8
0.0578  (132)
0.748  (0.339)
 .253  (.126)

    -19.6
                                                                                                                           Average
 24.1  (0.681)
    1.53
 102  (38.7)
1507  (0.711)
1610  (0.760)
   106.7
2.33  (2.11)
     64.0
    79.3
0.0507  (116)
0.656  (0.297)
 .294  (.146)
    93.
0.0597
0.771
 .343
3
 (137)
(0.350)
(.172)
                                                                   15.2
'Dry Standard Cubic Feet § 70°F, 29.92 in Hg
2Dry Standard Cubic Feet per Minute @ 70°F', 29.92 in Hg
3Actual Cubic Feed per Minute - Stack Conditions
''Normal Cubic Meters at 21.1°C, 760 mm Hg
5Metric Tons per Hour (1 metric ton = 1000 Kg)
6Grains per Dry Standard Cubic Feet

-------
                           Table 6 - SUMMARY OP RESULTS - OUTLET OF UNLOADING SEPARATOR CYCLONE - POINT 18
Run Number:

Date:

Method Type:
Volume of gas sampled-DSCFMNm3)11
Percent Moisture by Volume
Average Stack Temperature-°P-(°C)
Stack Volumetric Flow  Rate-DSCPM2-(Nm3/sec)
Stack Volumetric Plow  Rate-ACFM3-(m3/sec)
Percent Isoklnetic
Product Rate-ton lint  cotton/hr-(M  ton/hr)5
Duration of  run — minutes
Partlculates - probe,  cyclone
               and filter catch

mg
gralns/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton  produced
(kg/M ton of lint cotton produced)
.Partlculates - total catch

mg
gralns/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton  produced
(Kg/M ton of lint cotton produced)
percent implnger catch
                                                              18-1
                                                                                   18-2
  10-18-72

 EPA Method 5
21.5  (0.609)
 '   2.60
 109  (12.8)
1350  (0.637)
1480  (0.698)
    105.9
1.98  (1.80)
     64.0
    111.14
0.0798  (183)
0.923  (0.418)
. .466  (.232)
    125.6
0.0900  (206)
1.04  (.472)
 .521  (.262)

     42.3
  10-18-72
 EPA Method 5

22.5  (0.637)
    1.88
  96  (35.6)
1430  (0.675
1520  (0.717)
    104.8
2.04  (1.85)
     64.0
    114.7
0.0785  (180)
0.962  (0.436)
 .472  (.236)
    129.5
0.0886  (203)
1.09  (0.494)
 .531  (.267)

     11.4
                                              18-3
  10-19-72
 EPA Method 5
22.9  (0.648)
    2.76
  98  (36.7)
1460  (0.689)
1570  (0,741)
    104.6
2.96  (2.69)
     64.0
     65.8
0.0442  (101)
0.553  (0.251)
 .187  (.0933)
     93.3
0.0627  (143)
0'.785  (.356)
 .265  (.132)

     29.5
                                                                 Average
22.3

 101
1413
1523

2,33
  (0.631)
2.41
  (38.3)
  (0.667)
  (0.719)
 105
  (2.11)
 64.0
     97.3 .
0.0675  (155)
0.813  (0.368)
 .375  (.187)
    116.1
0.0804  (184)
0.972  (0.441)
 .440  (.220)

     27.7
 'Dry  Standard  Cubic  Feet  @  70°F,  29-92 In Hg
 2Dry  Standard  Cubic  Feet  per Minute  @  70°F,  29.92 in Hg
 3Actual  Cubic  Feed per  Minute - Stack  Conditions
 ••Normal  Cubic  Meters at 21.1°C, 760  mm Hg
 5Metrlc  Tons per Hour (1  metric ton  =  1000 Kg)
 6Gralns  per Dry Standard  Cubic Feet

-------
                                  Table 7 - SUMMARY OF RESULTS  - INLET  TO  INCLINED  CLEANER  CYCLONES -
co
Run Number:

Date:
Method Type:

Volume of gas sampled-DSCF^CNm3)1*
Percent Moisture by Volume
Average Stack Temperature-°F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(Nm3/sec)
Stack Volumetric Flow Rate-ACFM3-(m3/sec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes

Particulates - probe, cyclone
               and filter catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
                                                                   10-1
                                                                 10-16-72
                                                             High Vol.  Sampler

                                                                491  (13-91)
                                                                   6.34
                                                                163  (72.8)
                                                               2486  (1.17)
                                                               3103  (1-47)
                                                                    116
                                                               2.33  (2.11)
                                                                   12.0
   64717.8
2.03  (4647)
43-3  (19.6)
18.6  (9.29)
                                                                                        10-2
                                                                                               POINT 10

                                                                                                      10-3
                       10-16-72

                   High Vol.  Sampler
                      236   (6.68)
                         4.55
                      163   (72.8)
                     2380   (1.12)
                     2914   (1.38)
                          117
                     1.88   (1.71)
                          6.0
   44798.8
2.93  (6707)
59.7  (27.1)
31.8  (15.8)
                       10-17-72
                   High Vol.  Sampler
                      241   (6.81)
                         3.02
                      150   (65.6)
                     2810   (1.33)
                     3328   (1.57)
                          101
                     1.37   (1.24)
                          6.0
   24987-5
1.60  (3662)
38.5  U7-5)
28.1  (14.1)
                                                                                                                               Average
                     322

                     159
                    2559
                    3115

                    1.86
      (9-13)
    1.64
      (70.4)
      (1.21)
      (1.47)

      (1.69)
   44834.7
2.15  (4921)
47.2  (21.4)
26.2   13.1)
       'Dry  Standard Cubic Feet @ 70°F,  29.92 in Hg
       2Dry  Standard Cubic Feet per Minute @70°F, 29-92 in Hg
       3Actual  Cubic Feed per Minute - Stack Conditions
       ••Normal  Cubic Meters at 21.1°C, 760 mm Hg
       5Metric  Tons  per Hour (1 metric ton = 1000 .Kg)
      .6Grains  per Dry  Standard Cubic Feet

-------
                           Table 8 - SUMMARY OF RESULTS - OUTLET OF INCLINED CLEANER CYCLONES  -  POINT  1
Run Number:

Date:

Method Type:

Volume of gas sampled-DSCF^CNm3)1*
Percent Moisture by Volume
Average Stack Temperature-0F-(°C)
Stack Volumetric Plow Rate-DSCFM2-(Nm3/sec)
Stack Volumetric Flow Rate-ACFM3-(mVsec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes

Particulates - probe, cyclone
               and filter catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/tbn of lint cotton produced
(kg/M ton of lint cotton produced)

Particulates - total catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
percent impinger catch
                                                             1-1
                                                                                 .4-2
                                              4-3
                                                                                                                         Average
  10-16-72

 EPA Method ^
30.0  (0.849)
     6.34
 124  (51.D
1920  (0.906)
2240  (1.06)
    104.5
2.33  (2.11)
     64.0
     74.4
0.0382  (87.4)
0.629  (0.285)
 .270  (.135)
     99.1
0.0509  (116.5)
0.838  (0.380)

  .360  (.180)
     24.9
  10-16-72

 EPA. Method 5

31.8  (0.900)
     4.56
 121  (49-4)
2060  (0.972)
2350  (1.11)
    102.8
1.88  (1.7D
     64.0
     52.2
0.0253  (57-9)
0.447  (0.203)
 .238  (.119)
     69.1
0.0335  (76.7)
0.591  (0.268)

  .314  (.157)
     24.5
  10-17-72

 EPA Method 5

32.8  (0.929)
     3.02
  97.  (36.1)
2090  (0.986)
2250  (1.06)
    104.7
1.37  (1.24)
    . 64.0
     52.4
0.0246  (56.3)
0.441  (.200)
 .322  (.161)
     67.0
0.0315  (72.1)
0.564  (0.256)

  .412  (.206)
     21.8
31-5

 114
2023
2280

1,86
 (0.893)
4.64
 (45.6)
 (0.955)
 (1.08)
104
 (1.69)
64.0
     59.7
0.0294  (67.2)
0.506  (0.229)
 .277  (.139)
     78.4
0.0387  (88.4)
0.664  (0.301)

  .363  (.181)
     23-7
'Dry Standard Cubic Feet S 70°F, 29-92  in Hg
2Dry Standard Cubic Feet per Minute @ 70°F, 29-92  in Hg
3Actual Cubic Feed per Minute - Stack Conditions
"Normal Cubic Meters at 21.1°C, 760 mm  Hg
5Metrlc Tons per Hour (1 metric ton = 1000 Kg)
6Grains per Dry Standard Cubic Feet

-------
                                   Table  9  -  SUMMARY  OF  RESULTS  -  INLET TO EXTRACTOR FEEDER, GIN STAND CYCLONES - POINT 8
[\J
O
Run Number:

Date:

Method Type:

Volume of gas sampled-DSCF^CNm3)1*
Percent Moisture by Volume
Average Stack Temperature-°F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(Nm3/sec)
Stack Volumetric Flow Rate-ACFM3-(m3/sec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes

Particulates - probe, cyclone
               and filter catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
                                                                     3-2
                                                                                                              8-4
                                                                   10-13-72

                                                               High Vol.  Sampler

                                                                 73-9   (2.09)
  90
3110
3250

1.86
                                                                       (32.2)
                                                                       (1.17)
                                                                       (1.53)
                                                                      112
                                                                       (1.69)
                                                                      1.5
   31331.3
6.54  (15000)
 174  (78.8)

93.5  (46.6)
                       10-16-72
                   High Vol.  Sampler

                      125   (3-55)
 111
3030
3320

1.63'
.42
 (43-9)
 (1.43)
 (1.57)
8.1
 (1.48)
3.0
   45395-3
5.59  (12800)
 145  (65.7)

89.0  (44.4)
    10-16-72
High Vol. Sampler

  33.8  (0.956)
      1.80
   111  (43.9)
  3040  (1.44)
  3310  (1.56)
      78.9
  1.88  (1.7D
       1.0
                   17215.3
                7.87  (18000)
                 205  (92.9)

                 109  (54.3)
                                                                                                                                 Average
77-7  (2.20)
    1.95
 104  (40)
3060  (1.44)
3293  (1.55)
    96.3
1.79  (1.63)
     1.83
                         31314.0
                      6.22  (15300)
                       175  (79.2)

                      97.2  (48.4)
        'Dry  Standard Cubic Feet @ 70°F,  29-92 in Hg
        2Dry  Standard Cubic Feet per Minute @70°F, 29-92 in Hg
        'Actual  Cubic Feed per Minute - Stack Conditions
        ••Normal  Cubic Meters at 21.1°C, 760 mm Hg
        5Metric  Tons per Hour (1 metric ton = 1000 Kg)
        6Grains  per Dry Standard Cubic Feet

-------
                           Table 10 - SUMMARY OF RESULTS - OUTLET OF EXTRACTOR FEEDER,  GIN STAND CYCLONES  - POINT  6
Run Number:

Date:

Method Type:

Volume of gas sampled-DSCFMNm3 )*
Percent Moisture by Volume
Average Stack Temperature-°F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(NmVsec)
Stack Volumetric Plow Rate-ACFM3-(m3/sec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M  ton/hr)5
Duration of run - minutes

Partlculates - probe, cyclone
               and filter catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(kg/M ton of lint cotton produced)

Particulates - total catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
percent impinger catch
                                                             6-1
                                                                                 •6-2
  10-12-72
 EPA Method 5

52.6  (1.49)
    1.65
 111  (43.9)
1390  (0.656)
1500  (0.708)
    108.0
1.86  (1.69)
    64.0
    138.8
0.0406  (92.9)
0.484  (0.220)
 .260  (.130)
    152.6
0.0447  (102)
0.532  (0.241)

  .286  (.143)
     9.04
  10-16-72
 EPA Method 5
40.4  (1.14)
    2.42
  95  (35)
1080  (0.5098)
1150  (0.543)
    106.7
1.63  (1.48)
    64.0
     60.8
0.0232  (53.1)
0.215  (0.098)
 .132  (.0662)
     77-1
0.0294  (67.3)
0.272  (0.123)

 .167  (.0831)
     21.1
                                              6-3
  10-16-72
 EPA Method 5

45-5  (1.29)
    1.80
  96  (35.6)
1250  (0.590)
1320  (0.623)
    104.3
1.88  (1.71)
    64.0
     39.4
0.0133  (30.4)
0.142  (0.064)
 .0755 .(.0374)
     60.5"
0.0205  (46.9)
0.220  (0.100)

 .117  (.0585)
     34.9
                                                                                                                         Average
46.1  (1.31)
    1.96
 101  (38.2)
      (0.585)
      (0.624)
     106
      (1.63)
1240
1323
1.79
    64.0
     79-7
0.0257  (58.8)
0.282  (0.127)
 .156  (.0779)
     96:7
0.0315  (72.1)
0.343  (0.155)

 .190  (.0949)
     21.7
'Dry Standard Cubic Feet @  70°F,  29.92  in Hg
2Dry Standard Cubic Feet per Minute @ 70°F, 29.92 in Hg
3Actual Cubic Feed per Minute - Stack Conditions
'•Normal Cubic Meters at 21.1°C, 760 mm  Hg
5Metric Tons per Hour  (1 metric ton = 1000 Kg)
6Grains per Dry Standard Cubic Feet

-------
                                  Table  11  -  SUMMARY  OF  RESULTS  -  INLET TO BATTERY CONDENSER FILTER - POINT 16
rv>
Run Number:

Date:

Method Type:
Volume of gas sampled-DSCF'-CNm3 )'*
Percent Moisture by Volume
Average Stack Temperature-°F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(Nm3/sec)
Stack Volumetric Flow Rate-ACFM3-(m3/sec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes
Particulates - probe, cyclone
               and filter catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
                                                                    16-1
                                                                                         16-2
                                                                                                       16-3
                                                                  10-10-72

                                                              High Vol.  Sampler
                                                                2870
                                                               15608
                                                               17917

                                                                1.72
    (81.3)
   2.0
.7   (31.5)
    (7.36)
    (8.46)
   95
    (1.56)
   iO.O
                                                                   12045.7
                                                               0.065   (148.8)
                                                                8.61   (3.91)
                                                                5.00   (2.50)
                     10-10-72

                High Vol.  Sampler
 2948

 92.5
15880
16743

 1.64
 (83.5)
2.0
 (33.6)
 (7.49)
 (7.9)
80
 (1.49)
10.0
                      11863.1
                  0.062   (141.9)
                   8.44   (3.83)
                   5.15   (2.58)
    10-11-72
High Vol. Sampler

  3295  (93.3)
                                                              Average
  87.7
 15781
 16412

  1.70
 2.0
  (30.9)
  (7.45)
  (7.75)
 82
  (1.54)
82.0
                         17^04.8
                     0.082  (187.7)
                      11.0  (4.99)
                      6.47  (3.21*)
 3038  (86.0)
      2.0
 89.63  (32.0)
15756  (7.44)
17024  (8.04)
     80.67
 1.69  (1.53)
     80.7
                                       13771.2
                                   0.0697  (159-5)
                                    9.35  (4.24)
                                    5.5t  (2.77)
       MJry  Standard  Cubic Feet % 70°F,  29-92 in Hg
       2Dry  Standard  Cubic Feet per Minute @70°F, 29.92 in Hg
       3Actual  Cubic  Feed per Minute - Stack Conditions
       ''Normal  Cubic  Meters at 21.1°C, 760 mm Hg
       5Metric  Tons per Hour (1 metric ton = 1000 Kg)
       6Grains  per Dry  Standard Cubic Feet

-------
                                   Table 12 - SUMMARY OF RESULTS  -  OUTLET OF BATTERY  CONDENSER FILTER - POINT 17
ro
OO
Run Number:

Date:

Method Type:

Volume of gas sampled-DSCF^Nm3)1*
Percent Moisture by Volume
Average Stack Temperature-0F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(Nm3/sec)
Stack Volumetric Flow Rate-ACFM3-(m3/sec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes

Partlculates - probe, cyclone
               and filter catch

mg,
gralns/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(kg/M ton of lint cotton produced)

Particulates - total catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
percent impinger catch
                                                                                         •17-2
                                                                                                              17-3
                                                                                                                                 Average
10-10-72
EPA Method 5
70.3 (1.99)
1.86
n't (15.6)
71tO (3-37)
7730 (3-65)
98.0
1.72 (1.56)
80
178.8
0.0392 (89.7)
2.40 (1.09)
10-10-72
EPA Method 5
44.5 (1.26)
0.0
101 (38.3)
7560 (3.57)
7850 (3-70)
101.4
1.64 (1.49)
80
127.0
0.0440 (101)
2.85 (1.29)
10-11-72
EPA Method 5
47.2 (1.34)
0.5
103 (39.1)
7910 (3.73)
8250 (3.89)
102.7
1.70 (1.54)
80
105.8
0.0345 (78.9)
2.34 (1.07)


54.0 (1.53)
0.79
106 (41.1)
7537 (3-56)
7943 (3.75)
100.7
1.69 (1.53)
80
137.2
0.0392 (89.9)
2.51 (1.15)
                                                                 i. lo  (.699)
                                                                     191.5
                                                               0.0420  (96.1)
                                                                 2.57  (1.17)

                                                                 1.19  (.750)
                                                                      6.63
  1.74  (.866)
      153-5
0.0531  (122)
  3.41  (1.56)

  2.10  (1.05)
      17.3
                                                                                                           1.3.8   (.695)
      122.5
0.0400  (91.5)
  2.71  (1.23)

  1.59  (.799)
      13.6
                                           1.51   (.752)
     155.8
0.0450  (103)
 2.91  (1.32)

 1.73  (.866)
     12.5
        'Dry Standard Cubic Feet @ 70°F, 29-92 in Hg
        2Dry Standard Cubic Feet per Minute 6 70°F, 29.92 in Hg
        3Actual Cubic Feed per Minute - Stack Conditions
        ''Normal Cubic Meters at 21.1°C, 760 mm Hg
        5Metric Tons per Hour (1 metric ton = 1000 Kg)
        6Grains per Dry Standard Cubic Feet

-------
                                           Table 13 - SUMMARY OF RESULTS - OUTLET OF TRASH HOPPER CYCLONE  -  POINT  7
IV)
4=-
Run Number:

Date:

Method Type:

Volume of gas sampled-DSCFMNm3)*
Percent Moisture by Volume
Average Stack Temperature-°F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(Nm3/sec)
Stack Volumetric Flow Rate-ACFM3-(m3/sec)
Percent Isoklnetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes

Partlculates - probe, cyclone
               and filter catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(kg/M ton of lint cotton produced)

Particulates - total catch

mg
grains/DSCF6-(mg/Nm3)
lb/hr-(Kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
percent impinger catch
                                                                             7-1
                                                                           10-11-72

                                                                          EPA Method ^

                                                                         1(5.7  (1.29)
                                                                              0.72
                                                                           98  (36.7)
                                                                         3040  (1.43)
                                                                         3150  (1.49)
                                                                             100.3
                                                                         1.93  (1.75)
                                                                              64.0
      108.7
0.0366  (83.8)
0.954  (0.433)

 .494  (.247)
                                                                             128.2
                                                                       0.0432  (98.9)
                                                                         1.13  (0.513)

                                                                         .585  (.293)
                                                                              15.2
                                                                                  7-2
                         10-12-72

                        EPA Method 5

                       44.0  (1.25)
                            1.05
                        105  (40.6)
                       2900  (1.37)
                       3060  (1.44)
                           101.2
                       2.44  (2.21)
                            64.0
      138.9
0.0486  (111)
1.21  (0.549)

 .496  (.248)
                           152.0
                     0.0532  (122)
                       1.32  (0.599)
                                              Average
                      44.9
                         0
                       102
                      2970
                      3105
       (1.27)
       (39.6)
       (1.40)
       (1.47)
     100.8
 2.19  (1.98)
      64.0
                       .541
        (.271)
        8.6
     123.8
0.0426  (97.4)
1.082  (0.491)

  .495  (.298)
     140.1
0.0482  (110)
 1.23  (0.556)

 .563  (.282)
      11.9
                'Dry Standard Cubic Feet @ 70°F, 29.92 in Hg
                2Dry Standard Cubic Feet per Minute @ 70°F, 29.92 in Hg
                3Actual Cubic Feed per Minute - Stack Conditions
                ''Normal Cubic Meters at 21.1°C', 760 mm Hg
                5Metric Tons per Hour (1 metric ton = 1000 Kg)
                6Grains per Dry Standard Cubic Feet

-------
                                         Table  It  - SUMMARY OF RESULTS - EPA 5 and HIGH VOLUME SAMPLERS COMPARISON - POINT 18
ro
\s\
Run Number:

Date:

Method Type:
Volume of gas sampled-DSCP'-CNm3)1*
Percent Moisture by Volume
Average Stack Temperature-°F-(°C)
Stack Volumetric Flow Rate-DSCFM2-(Nm3/sec)
Stack Volumetric Flow Rate-ACFM3-(m3/sec)
Percent Isokinetic
Product Rate-ton lint cotton/hr-(M ton/hr)5
Duration of run - minutes
Particulates - probe, cyclone
               and filter catch
mg
grains/DSCF6-(mg/Nm3)
lb/hr-(kg/hr)
Ib/ton of lint cotton produced
(Kg/M ton of lint cotton produced)
                                                                                     18-4
                                                                                                                   18-4-H
                                                                                   10-19-72
                                                                     EPA Method 5  (modified for arsenic)

                                                                                 26.1  (0.739)
                                                                                     0.87
                                                                                 82.0  (27.8)
                                                                                 1660  (0.781)
                                                                                 1700  (0.802)
                                                                                     105-3
                                                                                 2.15  (1.95)
                                                                                     64.0
     71.2
0.0420  (96.1)
0.597  (0.271)
 .278  (.139)
                                  10-19-72
                             High Vol. Sampler

                                 837   (23.7)
                                   0.86
                                82.0   (27.8)
                                1477   (0.697)
                                1512   (0.714)
                                     111
                                2.15   (1.95)
                                   64.0
    5623.7
0.104  (238.1)
 1.32  (0.599)
 .614  (.3.07)
              *Dry Standard Cubic Feet @ 70°F, 29.92 in Hg
              2Dry Standard Cubic Feet per Minute @70°F, 29-92 in Hg
              'Actual Cubic Feed per Minute - Stack Conditions
              ''Normal Cubic Meters at 21.1°C, 760 mm Hg
              5Metric Tons per Hour (1 metric ton = 1000 Kg)
              "Grains per Dry Standard Cubic Feet

-------
                      SECTION III

           PROCESS DESCRIPTION AND OPERATION
PROCESS DESCRIPTION
The following describes the process equipment and materials
from which all emissions at subject plant are derived, and
identifies each of those sources with the specific device
being used to control emissions there from.

Reference is made to the drawings showing the plant flow
diagram Figure 2 and location of each emission control device
Figure 3*  Details on the individual items of process equip-
ment, mentioned in this process description, may be found
in the Handbook for Cotton Ginners, Agriculture Handbook
No. 260 (USDA), 1964.

Seed Cotton Unloading
Seed cotton is unloaded from trailers by means of telescoping
suction tubes.  The resulting air stream, containing seed
cotton, passes through ductwork to a rock trap, where heavy
impurties such as rocks and green bolls are removed, then
to the unloading separator, where air and seed cotton are
separated.  The air from the unloading separator (containing
impurities such as dust derived from the seed cotton) is
drawn through the unloading fan to Cyclone Sets Nos. 6 & 7
in parallel.
                          26

-------
                                                                                                                                            Cyclone Set 2
IV)
—3
             Unloading at Trailers
            (Telescope Suction Tube)
                                                                                                                                         Note: A separator (bypassed
                                                                                                                                             & not in use) was attached
                                                                                                                                             to the inclined cleaner.
                                                                                                                                             Its inoperative trash line
                                                                                                                                             connected to the duct line
                                                                                                                                             leading to Cyclone set 1.
            Cyclone Set 4
            Telescope
            Suet
^scope     X
ion Tube I  \*\
                       	TV
                                SV SC Overflow
                                                             2 SYSTEMS IN PARALLEL (See Note 2)
                                                                   C/clone Set 1 CD      Cyclone Set 5
                                                                                                                            Note 2:  A 3rd system was
                                                                                                                                  available, not equipped
                                                                                                                                  with an inline filter.
                                                                                                                                  (Condenser exhausted
                                                                                                                                  to atmosphere)
                                                                                                                                                 Inline FilterS
                    Screw Conveyor
                    with Dropper
                    and Glower
                                                                                                                     A Air
                                                                                                                     SC Seed Cotton
                                                                                                                     LC Lint Cotton
                                                                                                                     S Seed
                                                                                                                     T Trosh
                                                                                                                     NG Natural Gas
                      Figure   2.     Plant   Plow  Diagram  -  Cotton  Ginning  Plant,   Test  No.  72-MM-23

-------
                                                                           Unloading of SC Raw
                                                                           Material from Trailers
ro
CO
             Cotton Ginning
             Plant Bldg.
Cyclone Sets (7)
(numbered as
shown)
V
             Screw Convexor
             (rece iv ing tra sh
             from Cyclone Sets
             Nos, 1 thru 7)

                       Extractor Feeders, Gin Stands, Unit —Air
                       Lint Cleaners, (Stick-&-Green Leaf
                       Extractor (bypassed), Separator at Inclined
                       Cleaner (bypassed).
                                   Drier #2 Separator


                                      Inclined Cleaner
                                                                               Condenser Section of Condenser — Un it —
                                                                               •Saw Lint Cleaner
                                                                        Condenser Section of Condens er—Un it-
                                                                        Saw Lint C leaner
                                         Overflow Separator (bypassed)
                                        Saw Sections of Condenser—Un it — Saw
                                        Lint Cleaners
                                     #2
                                     o
                                             #3
                               o
                                                     #4
o-
                                                             »5
o-
                                                                   Unloading Separator
                                                                    #6
                                                                         ••-Ducts
                                                                           (See Note)
                                                                            #7
                                                       c>^*oT"
                                                      acuum Dropper1^
                                      Note:  Points at which ducts,
                                            to cyclones, leave the
                                            plant bldg. are not in
                                            the order shown.
                                                                                                     Battery Condenser  Q
                                           Inline Filters (3)
                                           (numbered as shown)
                                                        Trash House
                                                        Cyclone   •-
     Figure  3.    Location  of  Emission  Control  Devices  -  Cotton  Ginning  Plant,  Test  No.  72-MM-23

-------
Seed Cotton Drying and Cleaning
A stream of hot gases is formed as a fan draws ambient air,
from inside the plant, and forces it through Heater No. 1
where natural gas is burned and the resulting combustion
products mix with the air stream.

Part of the hot gas mixture thus formed flows through a duct
to the seed cotton outlet of the unloading separator, where
the seed cotton is entrained and carried through Tower Drier
No. 1 to the inclined cleaner.  Gases, containing trash, are
separated from the seed cotton in the inclined cleaner and
are drawn through a fan to Cyclone Set No.  3

A stream of hot gases formed in Heater No.  2, similar to
that formed in Heater No. 1, flows through a duct to the
seed cotton outlet of the inclined cleaner, where the seed
cotton is entrained and carried through Tower Drier No. 2
to the Drier No. 2 separator.  Gases containing trash are
separated from the seed cotton in that separator and are
drawn through a fan to Cyclone Set No. 2.  The seed cotton
from that separator is channelled by gravity flow into the
screw distributor, which carries it into the ginning system.

Ginning and Lint Cleaning
The screw distributor distributes seed cotton to two extractor
feeders which, in turn, feed it to one gin stand each, at
rates controlled to the gin stand capacity.  When the flow
of seed cotton from the screw distributor exceeds the total
of the intake rates of the extractor feeders, the excess
seed cotton flows into the overflow bin, from which it is
picked up, at a suitable time, by a telescoping suction tube
and routed again through the unloading separator and the
seed cotton drying and cleaning system then back to the screw
distributor.
                           29

-------
Part of the hot gas mixture from Heater No. 1 flows into the
two extractor feeders.  Air, containing trash, is drawn from
those extractor feeders into a duct having a vacuum, induced
by a fan, wherein it is carried in a gas stream to Cyclone
Set No. 1.  The same gas stream receives trash from other
sources which are shown in Figure 1, and which will be noted
in the following paragraphs.

Additional trash from the extractor feeders and trash from
the gin stands is carried by a screw conveyor to a vacuum
dropper, thence into the duct carrying the gas stream to
Cyclone Set No. 1.

Within the gin stands, lint cotton is separated from seed.
The seed is removed to an elevated seed house by means of a
screw conveyor, dropper, blower and ductwork.  The lint
cotton is carried in air streams through the unit-air lint
cleaners (one for each gin stand), then through condenser-
unit-saw lint cleaners (one for each gin stand), then to the
battery condenser.

Trash from the unit-air lint cleaners is carried by belt
conveyor to openings into the vacuum line to Cyclone Set
No. 1.  Air from the upper (condenser) section of each con-
denser-unit-saw lint cleaner (containing trash) flows through
ducts to a fan, thence to an inline filter.

An additional system consisting of an extractor feeder, a
gin stand, and lint cleaners (the same types as those just
mentioned) was available and was put into operation during
the last part of our test program.  An inline filter was
not available for this system; its condenser emissions were
exhausted directly to atmosphere.  Otherwise, this system
operated in parallel and in the same way as the two similar,
previously-operated systems.

                          30

-------
Air streams from the saw units of the condenser-unit-saw lint
cleaners (containing trash and motes) flow through a fan to
Cyclone Set No.  5.     .

Air from the battery condenser (containing trash)  flows
through a fan to Inline Filter No. 3.

Lint cotton from the battery condenser flows into  the baling
press where the  products, bales of lint cotton,  are formed.

As shown in Figure 3, air and trash from inline  Filters Nos.
1, 2 and 3 feed  into a duct, thence through a fan  to the
outlet of the vacuum dropper removing trash from the screw
conveyor under Cyclone Sets Nos.  1 through 7«  Thus, trash
from all inline  filters and cyclones is entrained  in a gas
stream that carries it to the cyclone atop the trash house.
The total trash  is thus collected in the trash house which
is elevated to facilitate periodic removal by dumping into
a trailer or truck.

PROCESS OPERATION
The following list shows typical and peak process  operation
parameters for the sampled cotton gin.

Normal plant operating schedule:
     10 hrs/day   (1 shift)
      5 days/week
     12 weeks/year, plus a few days for remnants.
     From October to December (ginning season).

Average plant operating capacity:
     70 bales of lint cotton produced/day (2 gin stands)
     90 bales of lint cotton produced/day (3 gin stands)
                          31

-------
     60,000 Ibs of seed produced/day (2 gin stands)
     70,000 Ibs of seed produced/day (3 gin stands)

Capacity is based on one 10-hour shift per day;  two  hours
downtime for maintenance; 9 bales per hour (2 gin stands
operating); 11 bales per hour (3 gin stands operating);
800 Ibs seed per bale lint cotton.  Downtime periods range
from a few minutes to several hours.

Peak plant operating capacity:*

     140 bales of lint cotton produced/day (2 gin stands)
     l80 bales of lint cotton produced/day (3 gin stands)
     120,000 Ibs of seed produced/day (2 gin stands)
     140,000 Ibs of seed produced/day (3 gin stands)
     *  Based on two 10-hour shifts per day; other factors
        same as listed under "Average plant operating
        capacity."

The gin manager provided the following information on
                          1
operation during sampling.  All seed cotton processed
during sampling was machine-picked upland-type cotton.
Weather prior to and during testing had been dry, causing
the seed cotton entering the gin to be as dry as it  ever
was (estimated at 3% by the gin manager) in previous ginning
seasons.  Because of the dry conditions, the seed cotton
contained more dust than usual.  Production rate would have
been about 30% higher had the moisture content been 8%.   The
natural gas-fired driers were in use during sampling; their
1 Extracted from "Trip Report-Bleckley Farm Service Company
  Cotton Ginning Plant", by William 0. Herring; November
  16, 1972.

                           32

-------
purpose, however, was mostly to fluff the cotton to facilitate
removing trash, rather than to reduce moisture content.

The ginning plant was originally designed by Lummus Cotton
Gin Company in 1961.  It was purchased used, moved to its
present site, and operated for the first time by the present
owners in 1972.  Recorded production data show that when the
gin operated smoothly, its production rate was about one
500-pound bale each seven minutes (9 bales per hour).
Sampling was conducted from October 10 through October 19.
From October 10 through 16 two gin stands were in use.  On
October 17 the third gin stand was put on line and was
operated intermittently.  The third gin stand was put to
full use on October 18 and 19.  Recorded data show that  the
production rate was not significantly changed by adding  the
third gin stand, indicating that production was limited  by
factors other than the number of operating gin stands.

Production data recorded by the EPA Project Engineer during
sampling is summarized in Appendix B (Operation results)
and the raw data is in the "Process and Production Data
Sheets" in Appendix D (Operating Data Log).
                          33

-------
                      SECTION IV

          SAMPLING AND ANALYTICAL PROCEDURES
LOCATION OF SAMPLING POINTS

There are two types of emission control devices at the
Bleckley Farm Service Company Cotton Gin; 3-42 inch in-
line filters controlling emissions from the battery con-
denser and the lint cleaner condensers and 15-34" cyclones
controlling emissions from the overflow separators, lint
cleaners, unloading separator, dryer separators, extractor
feeders, gin stands, and trash hopper.

The in-line filters were prepared for sampling by removing
the rain shields and installing a 44" ID horizontal duct
166" long on both outlets of the filter.  Sample ports were
cut in the ducts for a horizontal sample traverse and a ver-
tical upward traverse.  The ports were located 133" (3-02 D)
from the filter and 33" (.75 D) from the outside air, thus
requiring 40 sampling points.  The sample system was in-
stalled on the battery condenser (point No. 17» 1?A) and
on one of the lint cleaner condenser (points 14, l4A).  The
filter on the lint cleaner (14, l4A) was clogged and no
samples were obtained at this site (or the corresponding
inlet).  The inlet to the battery condenser filter was 29"
ID and sampling ports were cut 196" (6.75 D) from the build-
ing (beginning of straight run) and 70" (2.4 D) from the 90°
elbow into the filter.  This port location was a compromise

                          34

-------
between the sampling location and the available space for
scaffolding.  Twenty sampling points were required.   A
schematic of the in-line filter showing the sampling ducts
and important dimensions are given in Figure 4.

The fifteen cyclones were approximately 3^" in diameter with
outlets ranging in size from 16 to 17".  Each cyclone was
equipped with a rain cap which had been adjusted to  provide
the proper back pressure for proper separation efficiency.
The arrangement was not suitable for sampling as there was
cyclonic flow from the device and no suitable straight length
of pipe was available.  To solve these problems, the rain
cap was removed and replaced with an adapter to fit  the top
of the cyclone to a 16" ID 180° large radius sheet metal
return bend with a bend radius of 2.5 D or 40 inches.  The
return bend was connected to a straightening vane and then
to a length of 16" ID pipe.  This arrangement directed the
flow downward to allow sampling from lower scaffolding, and
the straightening vane greatly reduced the cyclonic  flow.
The straight length of duct provided ample distance  for the
flow to be stabilized after the straightening vane.   The
candy cane as installed on the cyclone was estimated (with-
out the contribution of the straightening vane) to be equal
to at least 54 feet of straight pipe.  This estimate is based
on data in "Industrial Ventilation" published by the American
Conference of Governmental Industrial Hygienists.

The straightening vanes were constructed of 20 gauge sheet
metal following the honeycomb design suggested in "Fan Engi-
neering" of the Buffalo Forge Company.  The design criteria
for the vane is to provide honeycomb squares of 7-5  to 15%
of the diameter with the vane length to be three times the
square size.
                          35

-------
UJ





3D......
T
20 Traverse
Points
<;
Tra
Poi


verse
nts
XX "~-H
t — 1;
1
o 17
A
Sampling
Ports


53 • 	




i'

i

T



7




\


(—

70

\
i

1
Y
C-.
Trash^
^^____ 	 	 Line
llf
T
o 1
16
Rain Shield
(Removed) ...
J
._ j
^Fot
Pul
i
1
.



196


133" 	 ^-33
0
or Traversing
ley Points
',




Inlet I
t
f"

29"
Gin
Building

                 Figure  :4.,  Schematic of In-Line Filter Showing  Ducts  and Sampling Ports

-------
As a compromise between meeting the criteria and construc-
tion technique, the size of the squares in the honeycomb
were 2.5" and the length of the vane 7.5"-  The final design
of the vane is shown in Figure 5.

A total of five candy cane units were constructed,  and these
were moved from one cyclone bank to the next for sampling.

Different adapters were used depending on the size  of the
outlet of the cyclone.  All adapter joints were sealed with
furnace tape to assure a leak tight seal.  The straight
length of duct after the straightening vane was 194" long
with 160" (10 D) from the vane to the ports and 3^" (2.1 D)
from the port to the atmosphere.  As the duct has suffi-
cient length, the minimum number of traverse point  (12) can
be used.  This number was further reduced to 8 as the duct
is less than two feet in diameter.  No traverse points were
chosen closer than 1 inch to the wall of the duct.

The inlets to the cyclones varied greatly in both diameter
of duct and length of straight run available to meet sam-
pling criteria.  The pertinent data is as follows:
Point No.
13
10
8
Inlet from
Unloading
Separator
Inclined
Cleaner
Extractor
Feeders,
etc .
Diameter of
Duct (inches)
15
12
12
Upstream
Distance
(inches)
90 (6D)
96 (8D)
96 (8D)
Downstream
Distance
(inches)
15 (ID)
72 (6D)
24 (2D)
No. of
Traverse
Points
16
8
8
                          37

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                          16



.




1



• I
'


.



1
1



1
1




r '
7.

u ,
Figure 5.  Diagram of Straightening Vane Construction
                         38

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The schematic diagram of the inlets and outlet of the
cyclone banks is given in Figures 6, 7, and 8.

During the testing program, it was found that blockage in
the bottom end of the cyclone would cause larger trash to
exit through the top of the cyclone, and quickly close off
the passages in the straightening vane, forcing the gin to
shut down.  Inspection ports were cut into the 180° bend
just above the vane for checking and clean-out.  These
ports were closed by sheet metal bonds during test runs.

Approximately one month prior to the beginning of the sam-
pling* program a subcontract was let to Snead's Sheet Metal
Shop in Macon, Georgia, to construct the ducts, elbows,
and straightening vanes.  These were transported to the gin
along with the necessary scaffolding and lumber.  Prior to
the first day of sampling, the ducts were erected in the
in-line filters and on several of the cyclones.  Men and a
boom truck were supplied by Snead's to move the ducting
from one cyclone to the next during the sampling program.

Sufficient electrical power was not available at this cot-
ton gin.  Ward's Electrical Service of Hawkensville,
Georgia, installed a 60 amp transformer to convert the
440 V gin voltage to 110 V, 60 hertz service required by
the sampling equipment.
SAMPLING PROCEDURES

The outlets from all of the control devices at the cotton
gin were sampled generally in accordance with" the Methods
given in the August 17, 19713 Federal Register.   One excep-
tion was the use of the wet bulb-dry bulb technique to
                          39

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     160"
      Sample_
      Ports ~
           34"
      1,18

(8 Traverse
   Points)
                                        Straightening
                                            Vane
                                                (16 Traverse
                                                   Points)
                   ^Trash
                    Line
                                                               GIN

                                                            BUILDING

                                                            15"
Figure 6.  Schematic Diagram of Outlet Ducts, 1, 18, 1A,
           ISA, and Inlet Duct 13

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  Sample
  Port,s-^
    4
  (8  Traverse
     'Points)
                                       	96"	*
                                       traightening Vane
                                      Sample
                                      Ports

                                         10

                                      (4 Traverse
                                       Points Used)
                                                     Enlet
Pp. !">•(-
J- W .!, O

 4A
                                                            12"
Figure 7.  Schematic Diagram of Outlet  Ducts  4  and HA,
           and Inlet Duct 10

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Gin
Building


      12"
                                        Straightening
                                            Vanes
•96"
       ZTiT ___L^ )
     L___LJL	JLX
         /
       Sample
       Port 8
                                               \
                   (8  Traverse
                      Points)
             Traverse"}!^!'^ j_
              Port s -^
                6A
                                                     o ample
                                             o
                                                     (8 Traverse
                                                        Points)
 Figure  8.   Schematic Diagram of Inlet Duct 8, and Outlet
            Ducts 6 and 6A

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obtain initial moisture levels,  rather than Method 4,  Deter-
mination of Moisture in Stack Gases.   The low moisture levels
(1-4$) and low stack temperatures (below 212°F)  permitted
the use of this deviation.

Method 5 of the Federal Register Methods was used to obtain
the emission rate of all sampled outlets.  During these
sample runs, any unsampled outlets in the same cyclone bank
or connected to the same control device were traversed to
obtain the velocity profile and stock temperature following
Method 2.  If it is assumed that the  loading in grains/stan-
dard cubic foot is the same at all outlets of the control
devices in one unit, the emission rate in Ib/hr would be a
function of the differences in velocity at the outlets.  The
loading in grains/cubic foot were obtained from the Method
5 data, and from the velocity traverse of the unsampled
ducts, the emission rate in Ib/hr can be calculated for
each individual outlet.

Run 18-4 was designed to accomplish two objectives.  First,
the water in the second impinger was  replaced with 100 ml
of 2% NaOH.  The combination of water in the first impinger
and sodium hydroxide in the second was to trap arsenic
acid.  The sampling train was operated in a normal manner.
The second objective of this run was  to provide a compari-
son of data obtained by Method 5 apparatus with the High
Volume sampler.  Run 18-4H, the High  Volume run, was con-
ducted simultaneously with run.18-4.

No conditions were encountered during this sampling pro-
gram that were beyond the normal operating parameters of
the Method 5 sampling apparatus.  The sampling runs were
stopped however when portions of the  gin ceased operation
                          43

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of if unusual conditions occurred in the gin.  The runs
were restarted when normal operation resumed.

A High Volume sampler designed and constructed by EPA was
used on the inlets to the control devices.   These inlets
usually contained large quantities of relatively large size
particulate matter.  In addition, the velocities in these
ducts were quite high.  Both of these factors made it im-
practical to attempt to sample the inlets with a Method 5
sampling train.

The High Volume sampler consisted of a 1-1/2 inch stain-
less steel probe and nozzle, a cyclone collector, a 8-1/8 x
10-1/2 inch filter holder for a 8-1/2 x 11 fiberglass filter
(MSA 1106 B) , a Roots meter, flow orfice, and the necessary
pump  and control devices.  Details of the sampler and the
equations relating to its use are given in Appendix E.

Sampling of the inlets with the High Volume apparatus was
conducted simultaneously with Method 5 sampling on the out-
lets to permit the calculation of efficiency data on the
control devices.  Sampling at Point 13, inlet to the unload-
ing separator cyclone and Point 16, inlet to the battery
condenser filter, were of the same time duration as the
corresponding outlets.  However, on Points 8, inlet to the
extractor feeder, gin stand cyclones, and 10, inlet to the
inclined cleaner cyclones, only very short runs were pos-
sible due to the extremely high loading levels in the inlet.
In these ducts, sampling times were made as long as possible
without completely filling the cyclone and filter.

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ANALYTICAL PROCEDURES

Samples from the Method 5 sampling trains were recovered as
outlined in the August 17, 1971, Federal Register.   After
removal of the filter, all sample exposed surfaces  were
washed with reagent grade acetone or distilled water as
specified.  All sample bottles for liquid samples were ob-
tained from Wheaton Scientific, Catalogue No.  219630.  Each
of these bottles and the petri dishes for sample filters
were acid soaked with 1:1 HN03 for one day,  rinsed  with
distilled water and soaked with distilled water for one day

Sample recovered from the High Volume sampler  included re-
moval of the filter and placing it in a large  mouth bottle,
removal of the cyclone bottle and sealing it,  and washing
of all exposed surfaces of the train with acetone.   Ace-
tone washings were placed in acid washed Wheaton bottles.

Analytical procedures for the Method 5 samples follow
the Federal Register guidelines, with one exception.  Con-
tainer No. 3 as indicated in the method contains water
from the impingers and washing of the glassware of  the
train.  The solution was extracted with chloroform  and
ether, and then the extracted portion was dried to  con-
stant weight, as specified.  In addition, the  remaining
water after extraction was evaporated to dryness at 212 °F
to constant weight.  Both weights were included in  the
total mass of particulate.

Sample weight from the Method 5 samplers were  reported as
"front half" (probe washings and filter collection  weights)
and "total" (front half plus water, chloroform-ether ex-
tract and impinger acetone washing weights).

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The analytical procedure for the High Volume sampler is sim-
ilar to the front half of the Method 5 procedure.   The filter
is dried to constant weight as is the dry cyclone  catch.
The acetone washing of the probe and all surfaces  up to the
filter were evaporated and dried to constant weight.  The
total particulate mass is the sum of the weight of the
three parts.

All dried samples from the runs were submitted to  the EPA.
Specific samples were analyzed pesticides, arsenic, and
trace metals.  The results are summarized in Appendicies
H, I, and J.

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