&EPA
            United States
            Environmental Protection
            Agency
            Office of Research and
            Development
            Washington, DC 20460
EPA/600/R-94/121B
July 1994
Blind-B Performance
Evaluation Study

A Statistical Evaluation of
the April 19,1994 Data
                                            0014rsd94.121b

-------
                 Blind-B
       Performance Evaluation Study
              April 19, 1994
      Environmental Protection Agency
Environmental Monitoring Systems Laboratory
            Las Vegas, Nevada

-------
            UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
                        OFFICE OF RESEARCH AND DEVELOPMENT
               ENVIRONMENTAL MONITORING SYSTEMS LABORATORY-LAS VEGAS
                                  P.O. BOX 93478
                            LAS VEGAS, NEVADA 89193-3478
                                   (702/798-2100)
Dear Participant,

   Enclosed are the results of the Nuclear Radiation Assessment Division (EMSL-LV)
Performance Evaluation Study for Blind-B; April 19, 1994.

   The known value for each analysis was determined by gravimetric methods,
checked by chemical analyses performed by EMSL-LV's Radiochemistry Laboratory,
and compared to the participating laboratories' grand average.
   The expected precision, determined by the known value, was taken from
"Table 3. Laboratory Precision:  One Standard Deviation Values and Control Limits
for Various Analyses", which is based on data accumulated over the years by the
Performance Evaluation Program, and can be found in the Environmental Radioactivity
Performance Evaluation Studies Program and Radioactive Standards Distribution
Program information brochure.

   Please take a few minutes to review this report and the analytical data your
laboratory submitted to us.  If there are any apparent discrepancies, please notify us
immediately.
   We encourage you to make use of the computer-automated data-entry system
that has been in place for some time now.  As the number of participants increases,
and it becomes unrealistic for us to receive results by mail or FAX, the computer
system will be our only avenue for accepting data.

   If you have any questions or comments, please send a message via the data-entry
system or contact George Dilbeck at 702/798-2104 or Patricia Honsa at 702/798-2141.
                                          Sincerely,
                                          George Dilbeck
                                          Chemist
                                          Radioanalysis Branch
Enclosure

-------
               NOTICE

This material has been funded wholly by
the U.S. Environmental Protection Agency.
It has been subject to the Agency's review,
and has been approved for publication as
an EPA document.

-------
               EMSL-LV Performance Evaluation: Blind-B,  19-Apr-1994             1 / 50


   The following pages consist of separate sections for each of the nuclides in this study with four
parts per section.  After the first, each part is separated from the next by a new page or a thick
horizontal bar.  The first page of each section is a statistical summary for the nuclide and starts
with a statement of the known value, the control limits, and the warning limits.

   The warning limits are placed at two normalized standard deviations above and below the
known value and the control limits are three normalized standard deviations above and below
the known value.  If you keep control charts, these values will be useful for anticipating problems
with the accuracy of your analytical methods.

   The coin shaped pie chart at the top of the summary page shows the fate of all the samples
sent out in number and percentage terms. The pie chart starts at the top and rotates clockwise.
The first sector represents those participants who submitted analytical results within both the
warning and control limits. The next sector represents those who are in the warning region but
not out of control. The third sector represents those who are out of control, but have passed
the outlier test. The fourth sector represents those who have failed the outlier test. The last
sector represents those participants who have failed to respond properly. This is the case if no
analytical results were returned, or less than three determinations were reported, or if the results
were received too  late. The reeding on the edge of the coin is spaced at one percent intervals, and
the sector shading becomes darker as the data reliability decreases. Sectors with zero width are
not shown.

   The table in the center shows a number of statistical quantities calculated from the submitted
data based on the mean and median values in relation to the known value, both before and after
outlier removal. The lower pie chart uses the same construction as the upper chart and shows
the distribution of properly submitted data in terms of deviation from the known value divided
into sectors representing one, two, three, and greater than three normalized standard deviations.

   The second part is an alphabetical listing, in lab-code order, of submitted data and several
calculated quantities. An entry that is shaded has been rejected because of one of the reasons
listed above or failure of the outlier test. The fifth and sixth columns are a measure of laboratory
precision. The Range analysis is a normalized value that you may use to keep precision control
charts. If this value is between 2.0 and 3.0, your analytical process precision is in the warning
zone; if it exceeds 3.0 it is out of control. The eighth and ninth columns are the differences from
the mean of all non-outliers and from the known value, respectively. A tag symbol may appear in
the last column. Each page with tags has a symbol definition summary at the bottom.  If there is
no tag symbol, the data is within the control limits, but it may be in the warning zone.

   The third part is a three-column listing of result average, tag symbol, and lab-code in average
order excluding those labs not responding properly. In this order, all outliers and out-of-control
results appear at the top or bottom of the list.

   The last part is two bar chart displays showing frequency distributions of responding
participants. The first chart places the known value at the center and a bar at each 0.2 unit of
expected precision. The second chart places the mean of the reported measurements at the center
and a bar at each 0.2 unit of standard deviation. In both cases,  a bar includes those results within
0.1 unit up to the maximum of six. Any results more than six units from the center value are
shown cumulatively by a shaded bar one past the sixth unit. If the central tendency of the known
value distribution falls away from the center, an error in accuracy is indicated. If the distribution
is broad, poor precision is indicated. The mean value distribution is similar but uses the average
and standard deviation of reported results as its basis.

-------
2/50            EMSL-LV Performance Evaluation: Blind-B,  19-Apr-1994
     The Range Analysis(R + SR) is calculated from the range, mean range and standard error of
  the range values.  The range is the difference between the maximum and minimum results for the
  laboratory. The mean range is calculated by multiplying the expected precision by 1.693(for three
  results).  The standard error of the range is calculated by multiplying the mean range by 2.575(for
  three results), subtracting the mean range from this product, and dividing the result by 3.  If the
  range is greater than the mean range, then the range analysis is calculated by subtracting the
  mean range from the range, dividing the result by the standard error of the range and adding 1.
  If the mean range is greater than or equal to the range, then the  range analysis is calculated by
  dividing the range by the mean range.

     The normalized deviation of the mean from the grand average is calculated from the deviation
  of the mean from the grand average and the standard error of the mean values.  The deviation of
  the mean from the grand average is calculated by subtracting the grand average from the
  average of the laboratory's three results. The standard error of the mean is calculated by
  dividing the expected precision by the square root of 3(the number of results). The normalized
  deviation of the mean from the grand average is calculated by dividing the deviation of the mean
  from the grand average by the standard error of the mean.
     The normalized deviation of the mean from the known value is calculated from the deviation of
  the mean from the known value and the standard error of the mean values.  The deviation of the
  mean from the known value is calculated by subtracting the known value from the average of the
  laboratory's three results.  The standard error of the mean is calculated by dividing the expected
  precision by the square root of 3(the number of results).  The normalized deviation of the mean
  from the known value is calculated by dividing the deviation of the mean from the known value by
  the standard error of the mean.
     A complete explanation of the statistical calculations involved in the report may be found in
  the Environmental Radioactivity Performance Evaluation Studies Program information brochure
  [Draft Revision of EPA-600/4-81-004], available from George Dilbeck, EMSL-LV, 702/798-2104.

-------
                 EMSL-LV Performance Evaluation:  Blind-B, 19-Apr-1994
                                     3/50
Gross Beta                          Statistical Summary                      216 Participants
The known value of this nuclide is 117.0 pCi/1 with an expected precision of 18.0; the control limits
are 85.8 to 148.2; the warning regions are 85.8 to 96.2 and 137.8 to 148.2
43(19.9 %) Failed to respond •«
5(2.3 %) Outliers '
18(8.3 %) Out of control'
      but not an outlier


        Statistic
                 129(59.7 %) Within all limits
  Respondents
• 21(9.7 %) In warning zone
         but within control


            Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
     441.79
    4387.42
19249479.28
     993.11
     277.60
       0.07
     108.33
       -7.41
       0.00
 Grand Avg 106.86
              15.47
             239.40
              14.48
              -8.67
              -0.66
             108.00
              -7.69
              -0.58
23(13.3 %) More than 3 norm. S.D


21(12.1 %) Between 2 and 3 norm. S.D
             .79(45.7 %) Within 1 norm. S.D.
                             of known value
       5O(28.9 %)
     »n 1 and 2 norm. S.D.

-------
4/50
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
Gross Beta
Lab
A
AA
AE
AF
AI
AJ
AK
AL
AO
AP
AR
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CF
CQ
CS
CX
D
DB
DD
DE
DG
DI
DL
DM
Res. 1
119.0
82.0
274:6
112.0

101.0
88.0
110.0
95.0
109.0
96.0
129.0
107.0

115.0
119.0
98.0
96.0
112.0

113.0
107.0
95.0
111.0
43.0
107.0
100.0
110.0
112.0
100.0
112.0

95.0

137.0
98.0
73.0
110.0
107.0
108.0
114.0
91.0

109.0
101.0
Res. 2
113.0
80.0
288.0
108.0
'"" \ "" % " •-
102.0
86.0
120.0
98.0
113.0
98.0
129.0
109.0
; ' - \
118.0
118.0
98.0
95.0
113.0

109.0
106.0
95.0
114.0
37.0
112.0
91.0
114.0
109.0
98.0
112.0
, ,< v
99.0

141.0
96.0
98.0
109.0
108.0
109.0
116.0
78.0

109.0
103.0
Res. 3
117.0
82.0
276.0,
110.0
" '" ',
95.0
92.0
110.0
103.0
106.0
95.0
129.0
105.0
, - ~ ;' -, -
118.0
119.0
97.0
95.0
112.0

111.0
108.0
90.0
115.0
93.0
113.0
112.0
117.0
107.0
110.0
119.0

91.0
'; ; y
139.0
94.0
72.0
110.0
109.0
108.0
117.0
81.0

109.0
106.0
• s No data submitted
0 s
Insufficient
data
x =
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
3.06
1.15
A 7*57
2.00
:•-,, • \
3.79
3.06
5.77
4.04
3.51
1.53
0.00
2.00
- *" < '• ..,-
1.73
0.58
0.58
0.58
0.58

2.00
1.00
2.89
2.08
30.75
3.21
10.54
3.51
2.52
6.43
4.04

4.00
'. "•
2.00
2.00
14.73
0.58
1.00
0.58
1.53
6.81

0.00
2.52
0.197
0.066
0.459
0.131
•-v * s ,
0.230
0.197
0.328
0.263
0.230
0.098
0.000
0.131

0.098
0.033
0.033
0.033
0.033

0.131
0.066
0.164
0.131
2.595
0.197
0.689
0.230
0.164
0.394
0.230

0.263
, f " ,-•
0.131
0.131
0.853
0.033
0.066
0.033
0.098
0.427

0.000
0.164
116.33
81,33
! 279.33
110.00
>" ''- -; ,
99.33
88.67
113.33
98.67
109.33
96.33
129.00
107.00
' '* ..' s ^
117.00
118.67
97.67
95.33
112.33
^ -.'''•• '' ' *
111.00
107.00
93.33
113.33
57.67
110.67
101.00
113.67
109.33
102.67
114.33
•' < ' " '•• '
95.00
>
139.00
96.00
81.00
109.67
108.00
108.33
115.67
83.33

109.00
103.33
TAG SYMBOLS
Determined to
be an
outlier
0.91
-2.46
1 10.66 -^
0.30

-0.72 v
-1.76
0.62
-0.79
0.24
-1.01
2.13
0.01
--', ., ",\ ,; \ '
0.93
1.14
-0.88
-1.11
0.53
' •:, -* '•" "' 's
0.40
0.01
-1.30
0.62
-4.73
0.37
-0.56
0.66
0^24
-0.40
0.72
,* ' ''* '-''••- * • '
-1.14
/-;\// ''},;:;'
3.09
-1.04
-2.49
0.27
0.11
0.14
0.85
-2.26

0.21
-0.34
11 == Above
U = Below
-0.06
-3.43 11
15'fl2;;'"*x;'
-0.67
•'' ,' -• '••••*
-1.70
-2.73
-0.35
-1.76
-0.74
-1.99
1.15
-0.96
'V;; ''.-»i"
0.00
0.16
-1.86
-2.08
-0.45
/•/J< 't •'''•"!
-0.58
-0.96
-2.28
-0.35
-5.71 U
-0.61
-1.54
-0.32
-0.74
-1.38
-0.26
^ ', -,- • '>
-2.12
":";? -v-:::^"
2.12
-2.02
-3.46 Ji
-0.71
-0.87
-0.83
-0.13
-3.24 li
( -" " " - •- ,
-0.77
-1.32
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
5/50
Gross Beta
Lab
DO
DS
DT
DZ
E
EB
EH
ELr
EO
r'EB'-
EV
EX;
FE
1 FF
FJ
FL
FN
FU
FZ
GE
GI
GQ
GT
GZ
HH
HI
HK
HL
HP
HU
HX
I
IA
1C
ID
IE
IU
J
JE
JG
JH
JN
JQ
JS
JY
• =
0 5
Res. 1
-
105.0
113.0
102.0
108.0
105.0
102.0
"", . "rf
115.0
° " \ - Xw * s ••
104.0
- , •• ^'JG;.
114.0
197.0 ..
139.0
93.0
103.0
87.0
75.0
109.0

117.0
97.0
138.0
-
110.0
106.0
116.0
89.0
146.0

103.0
- ' o - \ ," - 'I '
104.0
, x
104.0

119.0
131.0
117.0

99.0
154.0
95.0
96.0
Res. 2
- >v
104.0
112.0
110.0
113.0
112.0
103.0
•"%*J>.^\. \^* £,}£>'*
116.0
;^*i"^*^V>s"-"
103.0
i\"\x^^\r^>'
113.0
:"\ 197.0 ;•' '-'
137.0
98.0
104.0
92.0
75.0
109.0
'< ' - x >
124.0
102.0
137.0
v N
110.0
105.0
116.0
94.0
136.0
,lv\"v-^ iS v-v'Y-
105.0
"Ctv'v£":;j
106.0
'<- s
102.0

119.0
133.0
131.0

102.0
140.0
96.0
98.0
Res. 3
\
106.0
109.0
111.0
111.0
114.0
105.0
•-Osv «. V"" "•> ^
117.0
r *°'' : ' ' ^~
105.0
^,;,;;*;,;, -j
103.0

105.0

106.0
.'...,;.: ... '.:.
120.0
134.0
133.0

104.0
152.0
97.0
97.0
No data submitted
Insufficient
data
x =
Exper.
Sigma
X
1.00
2.08
4.93
2.52
4.73
1.53
, \ ^ * ""•
1.00
v < >->^; , ;, -
1.00
r - ^ ,s
1.00
7.61
7.00
2.89
3.21
2.65
10.39
0.00

7.00
3.61
1.53
^
0.00
1.00
0.00
4.04
5.03
""' . -, X , , ^
1.15

1.00

2.00

0.58
1.53
8.72

2.52
7.57
1.00
1.00
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag

0.066
0.131
0.295
0.164
0.295
0.098
,/,, ;-* 	 •.
0.066
' '"-."%:.
0.066
:; ' -/X \'- '
0.066
0^427
0.427
0.164
0.197
0.164
0.591
0.000

0.459
0.230
0.098

0.000
0.066
0.000
0.263
0.328

0.066
--,
0.066

0.131

0.033
0.098
0.525

0.164
0.459
0.066
0.066
S -~x-X%
105.00
111.33
107.67
110.67
110.33
103.33
'V "S^ v<.^>
116.00
'.>>'-'*;'•> ',-•'•- Y\- -}^
104.00
s - % "" -1"" X s -\ s -"-
114.00
142.00
96.33
101.67
90.00
81.00
109.00
- \ v
124.00
101.00
136.67
- s
110.00
106.00
116.00
93.33
140.67
' ""x^:v€:VK^
103.67
' "- ' .".-;:"'- ^'^
105.00

104.00

119.33
132.67
127.00

101.67
148.67
96.00
97.00
TAG SYMBOLS
Determined
to be an
outlier
" \s^: -^ v
-0.18
0.43
0.08
0.37
0.33
-0.34
-l-^f if ':>
0.88
,-i>x^,^ x,:^-'s
-0.27
^pfT ,-;;";.;
0.69
3.38
-1.01
-0.50
-1.62
-2.49
0.21
; v
1.65
-0.56
2.87
x \ w^
0.30
-0.08
0.88
-1.30
3.25
s^ip^-!^
:a3i_ _
»"lV'v^\^\»..<;
0.18

-0.27
<
1.20
2.48
1.94

-0.50
4.02
-1.04
-0.95
ft = Above
U = Below
X
-1.15
-0.55
-0.90
-0.61
-0.64
-1.32
F •' ,.-."'.•
-0.10
V. 	 , •'
-1.25
"."•'" -;,--«;
-0.29
2.41
-1.99
-1.48
-2.60
-3.46 I).
-0.77
<. *
0.67
-1.54
1.89
~ - •
-0.67
-1.06
-0.10
-2.28
2.28
^. i?' -^"' •
-1.28 	 ^
\$"%i:: "".".
-1.15
•
-1.25
.'. •:. ,. •?....
0.22
1.51
0.96
• :••'•
-1.48
3.05 ft
-2.02
-1.92
control limit
control limit
-^*

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6/50
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994

Gross Beta

Lab
K
KE
KM
KT
KX
L
LF
LG
LL
LR
LT
M
MA
.MN
MO
MP
MQ
MS
MV
MY
N
NA
NG
NH
-NT
NJ
NK
NO
NT
O

OF
OS
OX
OY
P
PA
PB
PC
PG
PI
PM
pp
PQ
PR
. =
0 s

Res. 1
79.0
103.0

20.0
116.0
116.0
99.0
111.0
81.0
113.0
100.0
144.0
121.0



116.0
'*' ' " '
117.0
i.
100.0
118.0
! ' v ' - - ; '
122.0
1 <
116.0
97.0
75.0
112.0
107.0

116.0
133.0
104.0
92.0
123.0
84.0
119.0
65.0
81.0

118.0

92.0
88.0

Res. 2
82.0
95.0

24,0;
119.0
115.0
110.0
113.0
, 89-°
102.0
100.0
140.0
116.0

' v •". f" "•

112.0

117.0

102.0
120.0
,-! ' * *
124.0

133.0
102.0
77.0
113.0
103.0

119.0
129.0
111.0
94.0
108.0
103.0
122.0
68.0
86.0

114.0

94.0
89.0

Res. 3
81.0
102.0

29.0
119.0
113.0
100.0
111.0
84.0
114.0
104.0
140.0
124.0
,


107.0

109.0

107.0
119.0
- ' ',' -'
114.0

125.0
105.0
79.0
112.0
111.0

120.0
129.0
114.0
94.0
119.0
98.0
120.0
71.0
80.0

112.0
„/
95.0
89.0
No data submitted
Insufficient
data
X s
Exper.
Sigma
1.53
4.36

4.51
1.73
1.53
6.08
1.15
4.04
6.66
2.31
2.31
4.04

••f^' ^

4.51
"s '•' :
4.62

3.61
1.00
''
5.29

8.50
4.04
2.00
0.58
4.00

2.08
2.31
5.13
1.15
7.77
9.85
1.53
3.00
3.21

3.06

1.53
0.58
Rnganal
(R + SR)
0.098
0.263

0.295
0.098
0.098
0.361
0.066
0.263
0.394
0.131
0.131
0.263


' - ' <
0.295

0.263

0.230
0.066

0.328
, '
0.558
0.263
0.131
0.033
0.263
/
0.131
0.131
0.328
0.066
0.492
0.623
0.098
0.197
0.197

0.197

0.098
0.033
Normalized deviation
Average
80.67
100.00

' 24.33
118.00
114.67
103.00
111.67
84.67
109.67
101.33
141.33
120.33
,


111.67
. '
114.33

103.00
119.00

120.00
^ *
124.67
101.33
77.00
112.33
107.00

118.33
130.33
109.67
93.33
116.67
95.00
120.33
68.00
82.33

114.67

93.67
88.67
TAG SYMBOLS
Determined
to be an outlier
(grand- eivg) (known) Tag
-2.52
-0.66

'• r>l94 '••''•"
1.07
0.75
-0.37
0.46
-2.14
0.27
-0.53
3.32
1.30

•',."' -/ ,
^ \ \" $ ~ ^ > *
0.46
, * • % '
0.72
/ , ""
-0.37
1.17
v r '' >
1.26
, , , - ' \
1.71
-0.53
-2.87
0.53
0.01

1.10
2.26
0.27
-1.30
0.94 -
-1.14
1.30
-3.74
-2.36

0.75
,- '• ' • • '" t
-1,27
-1.75
It == Above
II 52 Below
-3.50 II
-1.64
":;/" '. »
'', ,
-8.92 x!
0.10
-0.22
-1.35
-0.51
-3.11 II
-0.71
-1.51
2.34
0.32
v'v '•/-",' /•'"
-: !^/';":* :'
'x ''-> "• -'"•,* '
-0.51
* "* ~ - ? "' *
-0.26
*
-1.35
0.19
'' V ": -/ %•",'
0.29
•- ^ ' "" % : v
0.74
-1.51
-3.85 II
-0.45
-0.96

0.13
1.28
-0.71
-2.28
-0.03
-2.12
0.32
-4.72 II
-3.34 II
,' • - • •. •
-0.22
, *
-2.25
-2.73
control limit
control limit

-------

EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
7
/50
Gross Beta
Lab
PT
PV
PW
FT
Q
QC
QJ
QK
QL
QP
QQ
QT
QU
QW
QX
f\"U
t|Y\
QZ
RC
RD
RE
RF
RG
RJ
RK
RL
RM
RP
RR
RV
RZ
S
sc
SD
SF
SI
SL
SM
SO
SR
ss
ST
SW
sx
sz
T
Res. 1
63.0
104.0
•>'
', *-\ -
97.0
104.0
122.0
151.0
115.0
104.0
103.0
84.0
81.0
108.0


109.0
109.0
96.0
102.0
114.0
110.0
114.0


115.0

105.0
140.0
113.0
127.0
117.0
100.0
125.0
102.0
98.0
102.0
99.0
63.0
97.0
109.0
110.0
119.0
102.0
105.0
Res. 2
61.0
111.0
^ ' -.-X * ' ' ' \
Vs- - , "-, " " \ ;•
102.0
119.0
124.0
152.0
113.0
106.0
94.0
83.0
75.0
108.0
" •• -,; , "" *" v % ;• _"
•• '''"'* \ •• *• ^ \ v.
108.0
110.0
96.0
90.0
121.0
110.0
117.0
;\v :.^>j\
C , ', , . , ; "\
120.0
'£•'• ';,;; V-, r
105.0
118.0
107.0
127.0
118.0
104.0
96.0
94.0
101.0
103.0
98.0
67.0
101.0
92.0
112.0
104.0
122.0
101.0
Res. 3
57.0
103.0
"\ r ;7;" ''
;*. i^><:;
106.0
" -C-.--.0 -*1"
114.0
126.0
149.0
112.0
108.0
98.0
77.0
80.0
108.0

" ^0"
105.0
109.0
104.0
91.0
113.0
111.0
117.0
- - ,V - -
*>,. V"kSl
116.0
•- - :v;V
103.0
136.0
107.0
125.0
119.0
104.0
106.0
95.0
100.0
105.0
99.0
66.0
96.0
96.0
128.0
119.0
121.0
104.0
• 3 No data submitted
0 3
Insufficient
data
x =
Exper.
Sigma
3.06
4.36


4.51
\
7.64
2.00
1.53
1.53
2.00
4.51
3.79
3.21
0.00
•• * •>
A * ^ ^ s^> ^
2.08
0.58
4.62
6.66
4.36
0.58
1.73

%. ^ -t%.
2.65

1.15
11.72
3.46
1.15
1.00
2.31
14.73
4.36
1.53
1.53
0.58
2.08
2.65
8.89
9.87
8.66
11.27
2.08
Rnganal
(R + SR) Average
0.197
0.263
V. ^ ^ •.., ^
-,-; , \\/
0.295
0.492
0.131
0.098
0.098
0.131
0.295
0.230
0.197
0.000

11 •"• v \
0.131
0.033
0.263
0.394
0.263
0.033
0.098
-, .^, \

0.164

0.066
0.722
0.197
0.066
0.066
0.131
0.952
0.263
0.098
0.098
0.033
0.131
0.164
0.558
0.591
0.492
0.656
0.131
60.33
106.00
,"-' "--V;- ,-, - v*
>v! ; ~ ,' '-' :s" !' -,
101.67
112.33
124.00
150.67
113.33
106.00
98.33
81.33
78.67
108.00
t "" s A" w v^ '"" 5^

107.33
109.33
98.67
94.33
116.00
110.33
116.00
. ^-0 ~, ;~,
-': •/- '\ \\
117.00
~" ' ,*r~
104.33
131.33
109.00
126.33
118.00
102.67
109.00
97.00
99.67
103.33
98.67
65.33
98.00
99.00
116.67
114.00
115.00
103.33
TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known)
-4.48
-0.08
*V'>VV|^|^rf!"
v :A"*i^: iv^"
-0.50
0.53
1.65
4.22
0.62
-0.08
-0.82
-2.46
-2.71
0.11
- ^ 's '•^ •• "^ -. ^••'"l " ^ ^
V-, - ^ c* --\ ••'; *• f"1 h
0.05
0.24
-0.79
-1.20
0.88
0.33
0.88
i *\ _•, o^Xv11 i^.1"
;} ^iVt\'v^,-!?- -7?
0.98
,^v--rrx^-v^ -v-
-0.24
2.36
0.21
1.87
1.07
-0.40
0.21
-0.95
-0.69
-0.34
-0.79
-4.00
-0.85
-0.76
0.94
0.69
0.78
-0.34
tt = Above
& 3 Below
-5.45
-1.06
" l\-t\f"?s
•" N •" ^^s'> '
-1.48
-0.45
0.67
3.24
-0.35
-1.06
-1.80
-3.43
-3.69
-0.87
"V- "• \
, 	 - ss-^ ^
-0.93
-0.74
-1.76
-2.18
-0.10
-0.64
-0.10
-. -. V,s i "" ^ '
% __ ^
0.00
'""' "v "'"
-1.22
1.38
-0.77
0.90
0.10
-1.38
-0.77
-1.92
-1.67
-1.32
-1.76
-4.97
-1.83
-1.73
-0.03
-0.29
-0.19
-1.32
control
control
Tag
u

-; V"" ,
>. •-'
K™ '• -


tr



11
li

"*• •-••"' •.
- - • .







•• _ « ~-
X"" • ''

; •











11






limit
limit

-------
8/50
EMSL-LV Performance Evaluation: Blind-B,
19- Apr- 1994
Gross Beta
Lab
TA
TD
TE
TG
TH
TI
TL
TN
TQ
\TS" "
. m • •" -
TY
U
UA
UE
UG
UK
UN
UP
UQ
uw
UY
'VA"' "
vc
VG
VI '
VJ
Res. 1
68.0
128.0
118.0
97.0
110.0
100.0
119.0
116.0
106.0
170;0
i ''•''.'
95.0
106.0
105.0
120.0
141.0

137.0
111.0
105.0
88.0
82.0
\ '

92.0

99.0
VM 57740.0
m
vo
VT
W
WA
X
Z

120.0
112.0
99.0

108.0
104.0
Res. 2
66.0
98.0
120.0
100.0
103.0
94.0
119.0
112.0
111.0
" 159.0
% \ N
95.0
102.0
109.0
124.0
142.0
''": -* '"'',
121.0
121.0
104.0
96.0
87.0


96.0

112.0
57815.0

110.0
108.0
107.0

123.0
117.0
Res. 3
67.0
133.0
120.0
98.0
106.0
97.0
118.0
118.0
121.0
Exper.
Sigma
1.00
18.93
1.15
1.53
3.51
3.00
0.58
3.06
7.64
'', ' ' 170.•*

110.0
112.0
104.0
97.0
74.0

- , > V


98.0


93.0
57890,0


112.0
115.0
104.0
-:*'"'.,';

109.0
109.0
Data
Average
24.33
57.67
60.33
65.33
67.00
68.00







Tag
X
U
U
U
11
11
Lab
KT
BW
PT
SR
TA
PC
V"" y \\---: .
1.73
3.06
2.00
3.06
1.00
'V- '5 -
13.58
5.51
0.58
4.93
6.56

: ,':- =. • -
3.06
• ' ' -.
9.71
: , 75.30

5.29
3.51
4.04
•-\ "V *'>-'' V '
8.39
6.56
Rnganal
(R + SR)
0.066
1.283
0.066
0.098
0.230
0.197
0.033
0.197
0.492
OJ61
11 "!• •• ''
0.098
0.197
0.131
0.197
0.066
• '. •',
0.886
0.328
0.033
0.295
0.427

'• ' •;";»",. -
0.197
i '.
0.623
: 8:471
/
0.328
0.230
0.263
, ' --
0.492
0.427
Normalized
Average (grand-avg)
67.00
119.67
119.33
98.33
106.33
97.00
118.67
115.33
112.67
-3.84
1.23
1.20
-0.82
-0.05
-0.95
1.14
0.82
0.56
deviation
(known)
, ^4.81
0.26
0.22
-1.80
-1.03
-1.92
0.16
-0.16
-0.42
Tag
11








166,33^'' ^'<&i%] ^*{'*4>ilj"^"x\

'•-'", '' • '
96.00
102.67
107.00
120.67
141.00
1
,,* •
122.67
114.67
104.33
93.67
81.00


* *<• ^ -
' ;/>- f'.
95.33


101.33
:, /
-1.04
-0.40
0.01
1.33
3.29

1.52
0.75
-0.24
-1.27
-2.49

/ - ' '*-,-
-1.11
,*
-0.53
57815.00 5552,97


114.00
111.67
103.33


113.33
110.00

0.69
0.46
-0.34

0.62
0.30

-2.02
-1.38
-0.96
0.35
2.31
" ;••••••- •• -
0.55
-0.22
-1.22
-2.25
-3.46
' V

-2.08

-1.51
5551,99

-0.29
-0.51
-1.32

-0.35
-0.67
;' •>,





. :•"; , ,,




11
' ',•- -
".,•"•

- »'->

,"-"x\
'•



-• 9


sorted by Laboratory Average
Average






• = No data submitted
0 = Insufficient data
X
77.00
78.67
80.67
81.00
81.00
81.00
Tag
11
11
11
11
U
11
Lab
NO
QW
K
UY
FZ
CX
Average
81.33
81.33
82.33
83.33
84.67
88.67
TAG SYMBOLS
= Determined to be an outlier
Tag





,
U
11
11
U
U

ft s Above control
11 s Below control
Lab
QU
AA
PG
DG
LL
PR
limit
limit

-------


Gross Beta

Average
88.67
90.00
93.33
93.33
93.33
93.67
93.67
94.33
95.00
95.00
95.33
95.33
96.00
96.00
96.00
96.33
96.33
97.00
97.00
97.00
97.67
98.00
98.33
98.33
98.67
98.67
98.67
99.00
99.33
99.67
100.00
101.00
101.00
101.33
101.33
101.33
101.67
101.67
101.67
102.67
102.67
102.67
103.00
103.00
• = No data

EMSL-LV Performance

Data sorted
Tag Lab
AK
FU
OY
HP
BO
UW
PQ
RE
PA
CO
VG
BH
TY
JS
CS
FL
AR
TI
SI
JY
BG
ss
TG
QT
SO
RD
AO
ST
AJ
SL
KE
GT
CA
VJ
NK
LT
Q
JN
FN
U
SD
CJ
N
LF
Average
103.33
103.33
103.33
103.33
103.33
103.67
104.00
104.00
104.33
104.33
105.00
105.00
106.00
106.00
106.00
106.33
107.00
107.00
107.00
107.00
107.33
107.67
108.00
108.00
108.33
109.00
109.00
109.00
109.00
109.33
109.33
109.33
109.67
109.67
109.67
110.00
110.00
110.00
110.33
110.33
110.67
110.67
111.00
111.33

Evaluation: Blind-B, 19-Apr-1994

by Laboratory Average
Tag Lab
W
T
SM
EH
DM
I
IE
EV
UQ
RR
1C
DS
QQ
PV
HK
TH
UA
O
BN
AW
QZ
DZ
QX
DB
DD
SF
RZ
GE
DL
RC
CG
AP
OX
LR
D
Z
HI
AF
RG
EB
E
C
BM
DT
Average
111.67
111.67
111.67
112.33
112.33
112.33
112.67
113.33
113.33
113.33
113.33
113.67
114.00
114.00
114.00
114.33
114.33
114.67
114.67
114.67
115.00
115.33
115.67
116.00
116.00
116.00
116.00
116.33
116.67
116.67
117.00
117.00
118.00
118.00
118.33
118.67
118.67
119.00
119.33
119.33
119.67
120.00
120.33
120.33
submitted TAG SYMBOLS It &
0 = Insufficient data x s Determined to be an outlier U ==

9/50


Tag Lab
VT
MQ
LG
QJ
NT
BK
TQ
X
QP
BS
AL
CE
VO
sx
FE
MV
CK
UP
PM
L
SZ
TN
DE
RJ
RF
HL
EO
A
SW
P
RM
BA
SC
KX
OF
TL
BC
NA
TE
J
TD
NH
PB
MA
Above control limit
Below control limit

-------
10/50
               EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Gross Beta
Average
             Tag
                           Data sorted by Laboratory Average
                        Lab  Average       Tag        Lab  Average
                   Tag
                         Lab
  120.67
  122.67
  124.00
  124.00
  124.67
  126.33
  127.00
                        UE
                        UN
                        QK
                        GQ
                        NJ
                        S
                        JG
                                129.00
                                130.33
                                131.33
                                132.67
                                136.67
                                139.00
                                140.67
                                141.00
AU
OS
RV
JE
GZ
CQ
HU
UG
  141.33
  142.00
  148.67
  150.67
  166.33
  192.67
  279.33
57815.00
It
1t
x
x
x
x
M
FJ
JQ
QL
TS
FF
AE
VM
 % responding labs
                                 Frequency distribution
                 -4            -2            0            +2
                    Normalized deviation of the mean from the known value
                                                                                     &
% responding labs
10-	
                                  Frequency distribution
 0Jlm i
    -6
                  -4            -20            +2
                    Normalized deviation of the mean from the grand average
                                                                                     6
• = No data submitted
0 = Insufficient data
                                     TAG SYMBOLS
                              x = Determined to be an outlier
                                                                   It = Above control limit
                                                                   U = Below control limit

-------
                  EMSL-LV Performance Evaluation:  Blind-B, 19-Apr-1994
                                   11/50
Strontium-89                       Statistical Summary                      216 Participants
The known value of this nuclide is 20.0 pCi/1 with an expected precision of 5.0; the control limits
are 11.3 to 28.7; the warning regions are 11.3 to 14.2 and 25.8 to 28.7
121(56.O %) Failed to respond.
1(0.5 %) Outliers	
5(2.3 %) Out of control	
     but not an outlier

         Statistic
                ; 83(38.4 %) Within all limits

Respondents
6(2.8 %) In warning zone
       but within control

          Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value

Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
18.68
4.08
16.67
21.86
-6.61

-0.32
19.00
-5.00
-0.24
Grand Avg 18.49
3.69
13.58
19.93
-7.54

-0.41
19.00
-5.00 .
-0.27
6(6.3 %) More than 3 norm. S.D. «,
             56(58.9 %) Within 1 norm. S.D.
                           of known value
6(6.3 %) Between 2 and 3 norm. S.D.
     27(28.4 %) Between 1 and 2 norm. S.D.

-------
12 /
50
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Strontium-89
Lab
A
AA
AE
AF
AI
AJ
AK
AL
AO
AP
AR
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
CS
CX
D
DB
DD
DE
DG
DI
DL
DM
Res. 1
20.0
22.0
23.0
,
22.0
15.0
17.0
20.0
16.0
20.0
20.0
18.0

16.0

21.0
22.0

25.0
•.' * -.^ - •.

18.0
14.0
,,-. ,
16.0
19.0
23.0

. 17.0
9.0
11.0
26.0
19.0
25.0

16.0
17.0
19.0
•> X ,
v* ' * . • * * /<
Res. 2
21.0
25.0
23.0

25.0
15.0
22.0
- "•.""' * ^
V; ^<;1f',:'
23.0
17.0
18.0
17.0
19.0
w
17.0

21.0
26.0

23.0
>f" -
' ' V " '
19.0
14.0
-• , , -•* \
16.0
18.0
18.0
• , , :\,v ,-
7.0
8.0
11.0
25.0
12.0
24.0

16.0
17.0
19.0

1 ,' ' ' "'
Res. 3
20.0
•• \ ,^
23.0
23.0
', .
27.0
15.0
18.0
26.0
16.0
19.0
20.0
18.0

16.0
" t
16.0
24.0

23.0


21.0
17.0

14.0
20.0
19.0
' ; ' -VV'
12.0
5.0
11.0
21.0
15.0
26.0

17.0
18.0
15.0


• s No data submitted
0 5
Insufficient
data
X 3
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known)
0.58
1.53
0.00
'- * .
2.52
0.00
'2.65
" ^ " - ; ""
3.00
0.58
1.00
1.73
0.58
0.58

2.89
2.00

1.15


1.53
1.73
' : ' >
1.15
1.00
2.65
; " ^
5.00
2.08
0.00
2.65
3.51
1.00

0.58
0.58
2.31

__' * ' '<,'"'
0.118
0.354
0.000
V
0.591
0.000
0.591
0.709
0.118
0.236
0.354
0.118
0.118

0.591
0.473

0.236


0.354
0.354

0.236
0.236
0.591
<
1.345
0.473
0.000
0.591
0.827
0.236

0.118
0.118
0.473


20.33
23.33
23.00
"•' ^ I
24.67
15.00
19.00
23.00
16.33
19.00
19.00
18.33
16.33
- ' - \ , -\
19.33
24.00
'•:;-, J
23.67

} - * -. ' , f
19.33
15.00
* '. •• '
15.33
19.00
20.00

12.00
7.33
11.00
24.00
15.33
25.00

16.33
17.33
17.67
'

TAG SYMBOLS
Determined to
be an
outlier
0.64
1.68
1.56
s - -'- .-•'*" •':•
2.14
-1.21
0.18
1.56
-0.75
0.18
0.18
-0.06
-0.75
' ' *•?
0.29
1.91
- "-•-'' • ,-- ;, '
1.79

' ' M
0.29
-1.21

-1.09
0.18
0,52

-2.25
-3.87
-2.60
1.91
-109
2.25

-0.75
-0.40
-0.29

, V
1T = Above
!!• = Below
0:12
1.15
1.04
..' "', '
1.62
-1.73
-0.35
1.04
-1.27
-0.35
-0.35
-0.58
-1.27
:-f >^v/s
-0.23
1.39
/
1.27
'»*' ' "

-0.23
-1.73

-1.62
-0.35
0.00
? • "'•"" '
-2.77
-4,39
-3.12
1.39
-1.62
1.73

-1.27
-0.92
-0.81
, ,'


control
control
Tag
, ,;V;


•'*, -


.>:'



; V, v

' i, -


•• ,9

~i '•'
'"'• ' '


~" •:-



",S

u
Ji



*



• •
*
limit
limit

-------

EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
' 13 / 50
Strontium-89

Lab
DO
DS
DT
DZ
E
EB
EH
EL
EO
EH
EV
EX
FE
FF
F J

FL
FN
FU
FZ
GE
GI
GQ
GT
GZ
HH

m
HK

HL
HP
HU
ex
I

IA
1C
ID
IE
IU
J
JE
JG
JH
JN
JQ
JS
JY
• =
0 s

Res. 1
22.0

15.0
20.0
22.0
20.0
21.0
21.0
.'•• 1,
"• -. •- •- % "x

I"
21.0
~! .
\ * S ** "

' '° "'"' >l"
V - >">
23.0

I
A
12.0
x




18.0

~;
14.0
, 21.0

19.0


17.0



17.0
21.0




21.0
27.0

Res. 2
19.0
s.
13.0
20.0
19.0
21.0
19.0
18.0
':=t:' '• Y^s-'
-;<;;- //Y..
^YY^Y?'
vY ;;YSY
19.0
Y'if5~\\4<
YY~ Y' ty *••

YY:^ <.Y;;
r ;-;:-\:-V>-V;\
25.0
1 ,V Y\:SI,
~Yv>t '•*„
"• »'-YtY
12.0
>, _'"• ' ,
0 x ^ "" "
"•• „ j \ \ '^

"j / n
18.0

% "• ^ s ^v -.''
14.0
23.0
•:Y""-Y;4
21.0

"\ ;.\ J1- „.-'
18.0
• *


17.0
21.0




18.0
17.0

Res. 3
25.0
v
15.0
19.0
21.0
21.0
18.0
19.0
,'::;^\^': v
:!4 s !>x 7-'i % °
'\,\- *' '""' ~'"
v ^ s \ ^
20.0
";*'"?>L
s"\ vs ^ V '"•"-.% ^

'" v - \ \ '"•.
N\-^>^;-'-~ '"
25.0
% < ^
\ -v-.. "" $" '
*' -'*-' ' >
12.0
'.'-'>' * \«^ s-
v<:-. '^
*/ *<:••.'' -• < v ^

,-, -/ :- - r
18.0
* \ ^ •• ^ s

19.0
21.0
\cr-»-^" •'
21.0
"••• \^ ^ ^ t * s-^

17.0



17.0
20.0




17.0
16.0
No data submitted
Insufficient
data
XH
Exper.
Sigma
3.00
,
1.15
0.58
1.53
0.58
1.53
1.53
•!"• o
- s*NV ; °
, 5 V •-
^ \ 0

1.00
x >s * "" x



>• i..'.,^> _ • <•
1.15


•' '
0.00
v




0.00

'
2.89
1.15
,
1.15


0.58



0.00
0.58



,
2.08
6.08
Rnganal
(R + SR)
0.709

0.236
0.118
0.354
0.118
0.354
0.354
' '"'-;>" ,' !
t"" ^
,-' -- \ ^

0.236
^-- " ^" ,^-
'T


s r :•"•-
0.236
^ \


0.000





0.000


0.591
0.236
V '-.'"
0.236


0.118



0.000
0.118




0.473
1.570

Average
22.00

14.33
19.67
20.67
20.67
19.33
19.33
'l«j^\\:Yv-;;
' »<' ; * s ^;
/•\;t\^
-- ^;V^ ^Y-
20.00
' f -<-'!, V,*; ;
- ~!s's * J,""

T'rV ''^t
^- ^\-t*^--
24.33
^j v- •=• -"
^^^ *

12.00
- * -"* v~
••>-' '~v', '-^


\-~^ N~- ,,:--,
18,00

, . ' ' ^~\" -
15.67
21.67
HY \v*
20.33

~ ,, • > -'?",'.-
17.33



17.00
20.67




18.67
20.00
TAG SYMBOLS
Determined
to be an outlier
Normalized
(grand-avg)
1.21
* s< , \\ "
-1.44
0.41
0.75
0.75
0.29
0.29
^S'--Vx:-/ ?.-x^
"xV^Y^rV^ '
^ ^ --^ ^ - ," ^ ^
^^Ni'X ~ ,t'*V^V
0.52
i"k > >"- ^~ ^--"v ~y -
V\'':;- V~ V';\^: '

'7\ ^Y^v"'^,:
- ^'^s* *~ i'*"*;
2.02
;"<"-•>' • ^'-_ v ,•->••-• x^-
t;'^',\;/:rv
; V/'4^'""^vs>
-2.25
--vr-^V'
* ~ "». ",>*'"
--^X''\i'
•- ^^ ^5 ^ s^ ^ v
' ' X - "•' ^ '' ^K""
-0.17

' -• 'v-1' • " • ,
-0.98
1.10
w\x ' ^ V"^"^i-^\
"• ^x " £•• " * o ^ * ^ v ^ "V vv
0.64

' ' :~Y" , : c
-0.40



-0.52
0.75




0.06
0.52
deviation
(known) Tag
0.69
•
-1.96
-0.12
0.23
0.23
-0.23
-0.23
V7-.. *•'» ' ' •"
;\s \ / _-' '10 ' .
-v-. ;/' /•
>\;- ,,- ;~, »-
0.00
;\ ^ ,. -_V' • .
: *'~ . *** •

.-' - '-,,;, \' •. r
;--^,V>^-K ^«, -
1.50
^:; , ;\ :" , ,« -
;^': Y'^\/» '
-\ ' !- - ,
-2.77
' ;,^ ."•',,//••
\.-- ;' ~, ' , ;;••
- Iv x: ";-," '';: • x

,sl ' ^ -V- - •
-0.69

"•
-1.50
0.58
^":^;s^; :;, •
0.12

-, - .. •\1 '•
-0.92
x *
•
•
-1.04
0.23
• .
• • :
•
• .
-0.46
0.00
ft = Above control limit
Ji s Below control limit

-------
14 /
50 EMSL-LV
Strontiuxn-89
Lab Res. 1 Res. 2
K
KE
KM
KT
KX
L
LF
LG
LL
LM
LR
LT
M
MA
.MN
MO
MP
MQ
MS
MV
MY
N
NA
NG
NH
NT
NJ
NK
NO
NT
O
OF
OS
OX
OY
P
PA
PB
PC
PG
PI
PM
PP
PQ
PR
• =
0 =
9.0 10.0
20.0 18.0
22.0 22.0
20.0 21.0
18.0 19.0
17.0 18.0
20.0 19.0
15.0 19.0
18.0 18.0
20.0 19.0
20.0 20.0
8.0 9.0
18.0 22.0
20.0 21.0
No data submitted
Insufficient data
Performance Evaluation: Blind-B, 19-Apr-1994
Exper.
Res. 3 Sigma
10.0 0.58
19.0 1.00
22.0 0.00
18.0 1.53
18.0 0.58
19.0 1.00
19.0 ,,0.58
18.0 2.08
19.0 0.58
20.0 0.58
20.0 0.00
9.0 0.58
18.0 2.31
\
16.0 , 2.65
Rng anal
(R + SR) Average
0.118 9.67
0.236 19.00
0.000 22.00
0 \ \ / ' >
•••••. ' s l '
0.354 19.67
0.118 18.33
-. - ^
'v
0.236 18.00
0.118 19.33
0.473 17.33
0.118 18.33
0.118 19.67
0.000 20.00
0.118 8.67
0.473 19.33
0.591 19.00
TAG SYMBOLS
x = Determined to be an outlier
Normalised
(grand-avg)
-3.06
*•• \ ' i *" •• f *'' '-i *'•
0.18
1.21
- .. " / **• "• * J
0.41
-0.06
-0.17
0.29
-0.40
-0.06
0.41
0.52
-3.40
0.29
0.18

deviation
(known) Tag
^-3.58 |l
•>]!','> •,^s ; s^O ••''*> •"•• ••
-0.35
0.69
,-,- V,'-' ' ' *
-0.12
-0.58
' ' ! % '< l< * *
-0.69
, -' • - : s ',,'• »""
, *;y "<•;•>'' v
-0.23
>v,\ - ; y ; ' : V • •
-0.92
-0.58
-0.12
0.00
-3.93 U
-0.23
-0.35
tt = Above control limit
•li = Below control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
15/50
Strontium-89
Exper. Rng anal
Lab
PT
PV
PW
PY
Q
QC
QJ
QK
QL
QP
QQ
QT
QU
QW
, v'>r,'C
5 V- CT" ;:;.r->
23.0
30.0
-\ " -.
£•* ' " * v ,
<
10.0
23.0
\ " - ^
*•
19.0
19.0
* T~- - r! " ''A
Y'-r -.'/' " '-!
";-,, v >\i,j
" Vi s -
V --si


; -^ , ,, ^


16.0
, '• \. • ' ™\ "
19.0
15.0
\ s . y ' "• \ ^
18.0
18.0
23.0
" ., ' s ^
38.0

17.0


19.0
14.0


-
19.0
Res. 3
11.0
16.0
s >"*' " " '
V'S. V X
19.0
,-,v^
•? V"V ^x \ "
20.0
26.0
> <•
\\ s\
^
12.0
24.0
-
*
17.0
15.0
"• 1" "" S ^ ^
" s
•-''","' C \\v
\ ^ " ^ "






19.0
•J % ^ ', • -
18.0
16.0

19.0
16.0
14.0
* \
37.0

20.0
;-:" ' --• '

18.0
16.0



19.0
• = No data submitted
0 =
Insufficient
data
x =
Sigma (R
1.53
3.00
J -. $ "* ''
' ""- ' " - ' \
0.58


1.73
4.00
-


1.00
1.53
>

1.00
2.08



- ,- - - '

; , ,




2.52

0.58
0.58

1.53
1.15
4.93

2.65

1.73


2.08
1.53



0.58
+ SR)
0.354
0.709

- , ;: >
0.118

" - ' s "
0.354
0.945

\
t
0.236
0.354


0.236
0.473









:
0.591

0.118
0.118

0.354
0.236
1.120

0.591

0.354


0.473
0.354



0.118
Average
12.67
13.00
'v'i' ^'"-"^ '
.-;:>:>•. ' ,-'t:-
18.67
s s V
-\ .„. »v-^
21.00
26.00
<\
Vx
t '* N " '«* ]JxV
" "^ ^
11.00
22.67
<'
"
18.00
17.33
^ "^.~-- -'-:
V^\ ---'":; -c
x- X"!S- "
/V ' "•" Mli •••

- ' '""»'." ^

- '• h'


18.67

18.67
15.33
;""""•. 'v ,\
19.33
16.67
17.33
--
36.00

19.00


19.67
14.33



19.33
TAG SYMBOLS
Determined to
be an outlier
Normalized deviation
(grand-avg) (known) Tag
-2.02
-1.90
?;^}^^x
^>^;~ c^'^x ^
0.06
'^f '/ l'~Y *-?'V \v
sV-^.^r.vV" ;-
0.87
2.60
,^ >\^ :
VtV •* v
t
-2.60
1.45
s ^v \
vx *
* \
-0.17
-0.40
•• 'Ir^V^-^H
^V^>;^V':
-',--M>S; ; ;f;4^i;,y^'-
/-rr,(I%{:f;-V-:

,C;\1>> * % ?~v*? >
^V" o ^ ^^ s "-vr^V
V^ ,^,V;,\"!--/ // - .

' " -
°-06
;-.S
0.06
-1.09
, ,*" ,„•" ' --
0.29
-0.63
-0.40
>.
6.06

0.18


0.41
-1.44



0.29
ft s Above
•li s Below
-2.54
-2.42
*V:«V;, *
«
-0.46
"'"-x?«
' x - • "
0.35
2.08
,,•
•
v •
-3.12 U
0.92
x*
x - *
-0.69
-0.92
1 s~ •• s " "s
,;~-\" =, •\:"
1 x,V •
Y X' "-' -* •-'

';. ';W .- i- *
\x ^ s \^ ^
- r „ v • '

"- ' - •' •
-0.46
a
-0.46
-1.62
' - ;";- v . ; •
-0.23
-1.15
-0.92
X v •
5.54 x
•
-0.35
'. »K
'"••'
-0.12
-1.96
•
•
N •
-0.23
control limit
control limit

-------
r = 	 N.
16 / 50 EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
Strontium-89

Exper. Rng anal
Lab Res. 1 Res. 2 Res. 3 Sigma (R + SR) Average
•TA* ,.". -, -,.,-.. :> ,?': -
^ ^ "• ^ ' X " " "- ' ' •• "" J" s
TD 24.0 26.0 20.0 3.06 0.709 23.33
TEv •"., ; • ^V r-/ ;* --'
"TH'-' - -. • •• V'* - \ -

- '*" ' '-/ - •/"'* ! x
TI 16.0 16.0 18.0 1.15 0.236 16.67
TL 19.0 21.0 24.0 2.52 0.591 21.33
* -.-.>.- i •. * S •,-.., C ' * ^ '"•.•.'"
TN ' ' " - ;" ' , '-'---
"''•v'''''s*. i^V \ f < '

TQ 18.0 16.0 15.0 1.53 0.354 16.33
TS 16.0 15.0 17.0 1.00 0.236 16.00
TU . - ' > *— ' - .<* - , - ;<
TY, .- - : - > ' •- ; - - - ,
t
'/ s. '-" " ' ' ,V v -'-'> •"• ' V,
U 16.0 18.0 18.0 1.15 0.236 17.33
UA ' '* ": ' v '; " -' '-'-•' *
,- , * ,- „ , - - ' t ••- - : -, ,; ^ -r." -.,
UE 16.0 19.0 22.0 3.00 0.709 19.00
,UK v*' ",.'-'" *• " * -
UN , ' ' ' - , .. '-'. *


UP 17.0 14.0 19.0 2.52 0.591 16.67
UQ - . ' • :-':- "" -
'' " , '. '",''-'-;• - '• '
UW 27.0 29.0 29.0 1.15 0.236 28.33
UY \,*' - "• ';'': -/";
VC '' \ , " ^ , > , .'

- *
VG 19.0 18.0 16.0 1.53 0.354 17.67
vi '/ , ; - : / ,.--..
VJ ," , '•' ""'-'. ;
VM .>"->•- ••:• ;---; ;/
Vtf - ,' - \--'i , -'
vo --,''':."
~'VQ . "' . ' "- / ' ' ''" -
VT <\* *, Y ~^ Vy;

, ' '
--• , ;v -- ^ - ' - -, - • ' -- •-'
*-•:'; ',-: ,,*-••;
I
'• / '' ' -/" ' "-' 5 -
i =•'-,';' "-" '' \
W 17.0 18.0 18.0 0.58 0.118 17.67
WA . ' •;*' -i'^." - ''-
;'•'''.- '. ' ' ' ' ' ']''
X 21.0 21.0 20.0 0.58 0.118 20.67
Z 20.0 20.0 19.0 0.58 0.118 19.67
"
Normalized deviation
(grand-avg) (known) Tag
- v\ - ;• ^--'Cv-^''--'' -'-. »\:
1.68 1.15
• ,-''-": - VY'rY^v''^^;'
''•'._
-0.63 -1.15
0.98 0.46
.••.•.-.%• f^ v f. ^ f tt ^ ' * *
'- •"' °~% •
-0.75 -1.27
-0.86 -1.39
""'.," ^ ' f " ' '' * '' $ ",/• V'^1-^-.' •- "•
N-. " ' " , "" •
x- ,',; ',' •- ,'-»: '\'*>r\ ••• ,
-0.40 -0.92
^ - •• ••,.^f~- *'^:^~- *'";'>" *"\9t •'
0.18 -0.35
• ''*>' ~ W . * /'
•- . ' - „ - --'. '' "<\*
-0.63 -1.15
.. -,^~,~. ^: x-\,,^\;V;^v»- ;
3.41 2.89
'/-•"' '*- '• „*-•
- '• - *• -- /• ' *,-
-0.29 -0.81
' / ',,->•;' " .* ; '
" ' ,' -•- ; -,' '»- '
,;; -- , -'" /::^^--" ~-: ^; -
,, .~ -\ -;,--•-<'- :',"'- >-->-f ''
/ '\, . •
' / '' A !~!-' '''•'';'" *''\ *'••-
-'-, , ,'•,'„,',-, ;". •* -
-0.29 -0.81
, , ; - ' ; -;--;'"-v "'' •;-*•;"
0.75 0.23
0.41 -0.12
Data sorted by Laboratory Average
Average Ta£ Lab
7.33 Ji ' CP
8.67 H PC
9.67 U. K
11.00 li QU
11.00 U CQ
12.00 GQ
• = No data submitted
0 = Insufficient data
Average Tag Lab Average Tag Lab
12.00 CO
12.67 PT
13.00 PV
14.33 ST
14.33 DT
15.00 CA
TAG SYMBOLS
x = Determined to be an outlier
15.00 AK
15.33 RV
15.33 CX
15.33 CG
15.67 HP
16.00 TS
11 = Above control limit
11 s Below control limit

-------
EMSL-LV Performance Evaluation:
Strontium-89

Blind-B, 19- Apr- 1994

17 / 50 ]

Data sorted by Laboratory Average
Average Tag
16.33
16.33
16.33
16.33
16.67
16.67
16.67
17.00
17.33
17.33
17.33
17.33
17.33
17.33
17.67
17.67
17.67
18.00
18.00
18.00
18.33
18.33
18.33
18.67
18.67

% responding labs

10

-6 -4

• = No data submitted
0 5 Insufficient data
Lab Average Tag
TQ 18.67
DD 18.67
BH 19.00
AW 19.00
UP 19.00
TI 19.00
SC 19.00
J 19.00
U 19.00
SD 19.00
RC 19.33
NJ 19.33
1C 19.33
DE 19.33
W 19.33
VG 19.33
DG 19.33
QZ 19.33
MQ 19.67
HK 19.67
NO 19.67
M 19.67
BC 19.67
RR 20.00
RM 20.00
20.00
Lab Average
Q 20.00
JS 20.33
UE 20.33
SM 20.67
PQ 20.67
KX 20.67
CJ 20.67
BA 21.00
AZ 21.33
AL 21.67
T 22.00
S 22.00
PM 22.67
N 23.00
EL 23.00
EH 23.33
C 23.33
BL 23.67
Z 24.00
SS 24.00
NT 24.33
LT 24.67
DZ 25.00
PB 26.00
JY 28.33
FE 36.00
Tag Lab
CK
I
A
X
JE
EB
E
QK
TL
HU
L
DO
QW
AU
AF
TD
AE
BO
CS
BM
FU
AJ
D
QL
UW
x SI
Frequency distribution

B.._.
«...
ll.l
-2 0
Normalized deviation of the mean


Pmm .
+2 H
from the known value
TAG SYMBOLS ft =
x = Determined to be an outlier U =


—
-4 +6

Above control limit
Below control limit
...... -^

-------
18/50          EMSL-LV Performance Evaluation:  Blind-B,  19-Apr-1994
Strontium-89

 % responding labs	Frequency distribution
 10
     -6            -4            -2            0            +2            +4            +6
                    Normalized deviation of the mean from the grand average

-------
                                                                                     ,
                  EMSL-LV Performance Evaluation:  Blind-B,  19-Apr-1994
                                                  19/50
Strontium-90
Statistical Summary
                                     otciiisiiuai ouiiimary                       216 Participants
The known value of this nuclide is 14.0 pCi/1 with an expected precision of 5.0; the control limits
are 5.3 to 22.7; the warning regions are 5.3 to 8.2 and 19.8 to 22.7
113(52.3 %) Failed to respond •

1(O.5 %) Outliers	
         Statistic
                               10O(46.3 %) Within all limits
                                                                            •
               Respondents
                                                                       2(0.9 %) In warning zone
                                                                               but within control

                                                                                  Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
14.25
2.45
5.99
17.17
1.80
0.10
14.00
0.00
0.00
Grand Avg 14.13
2.14
4.59
15.15
0.96
0.06
14.00
0.00
0.00
1(1.O %) More than 3 norm. S.D
2(1.9 %) Between 2 and 3 norm. S.D. '
                           . 86(83.5 %) Within 1 norm. S.D.
                                           of known value
                   •14(13.6 %) Between 1 and 2 norm. S.D.

-------
20/50
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Strontium-90
Lab
A
AA
AE
AF
AT
AJ
AK
AL
AO
AP
AR
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
CS
CX
D
DB
DD
DE
DG
DI
DL
DM
• =.
0.3
Res. 1
13.0
14.0
12.0
13.0

17.0
16.0
15.0

<
„
15.0
17.0
14.0
14.0
14.0
13.0
15.0

13.0
16.0

12.0
13.0
15.0
15.0
17.0
13.0
17.0
, * '
11.0
7.0
13.0
17.0
15.0
14.0

15.0
16.0
11.0

•• •> •>'•• •>
Res. 2
14.0.
12.0
12.0
13.0

14.0
16.0
15.0



14.0
19.0
14.0
14.0
14.0
12.0
15.0
"*
13.0
17.0
, t '•• * •
12.0
13.0
14.0
12.0
17.0
13.0
18.0

16.0
8.0
11.0
16.0
15.0
14.0

14.0
16.0
14.0
,;,' ;';'-•
Res. 3
14.0
15.0
12.0
14.0
, x ! - -
17.0
16.0
15.0
' -. •• •• V ""-.

^ .. ''••', ""* '
15.0
, 17.0
14.0
15.0
14.0
11.0
15.0
' •'-'
16.0
15.0
" , ..
11.0
14.0
14.0
13.0
17.0
13.0
20.0
; '•;,';''•'"•-' -
15.0
12.0
13.0
18.0
16.0
14.0

15.0
17.0
13.0
•r * "
No data submitted
Insufficient
data
X 3
Exper.
Sigma
0.58
1.53
0.00
0.58

1.73
0.00
0.00
• ": ' ' ,
•'**', ''• "
?'-.' ; • -
0.58
1.15
0.00
0.58
0.00
1.00
0.00

1.73
1.00

0.58
0.58
0.58
1.53
0.00
0.00
1.53

2.65
2.65
1.15
1.00
0.58
0.00

0.58
0.58
1.53
*.
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
0.118
0.354
0.000
0.118

0.354
0.000
0.000


-:- i.
0.118
0.236
0.000
0.118
0.000
0.236
0.000

0.354
0.236

0.118
0.118
0.118
0.354
0.000
0.000
0.354

0.591
0.591
0.236
0.236
0.118
0.000

0.118
0.118
0.354

13.67
13.67
12.00
13.33

16.00
16.00
15.00
. '..- '-"' " •''
' '- > • * *\ **''•
'*' ' * s ' \. '
14.67
17.67
14.00
14.33
14.00
12.00
15.00
1 * * \ - -
14.00
16.00
, . ; \ - , <
11.67
V *"' "''- "
13.33
14.33
13.33
17.00
13.00
18.33

14.00
9.00
12.33
17.00
15.33
14.00
_..
14.67
16.33
12.67

,
TAG SYMBOLS
Determined
to be an
outlier
-0.16
-0.16
-0.74
-0.28

0.65
0.65
0.30


->",.v 'V\v
0.18
1.22
-0.05
0.07
-0.05
-0.74
0.30

-0.05
0.65
'.'•'• ,» - -*
-0.85
•',?;.>,:'•*''
-0.28
0.07
-0.28
0.99
-0.39
1.45
'' •, -. -. '• *
-0.05
-1,78
-0.62
0.99
0.42
-0.05

0.18
0.76
-0.51
' , -. ••
, :.•-''
It 3 Above
II s Below
-0.12
-0.12
-0.69
-0.23
•••- ' \ "* -
0.69
0.69
0.35
;V:" - - '/•<
, , "-' :: ' ••'
: . y. -' , ;. .
0.23
1.27
0.00
0.12
0.00
-0.69
0.35
•~:v -'.' »" ;
0.00
0.69
>' - ' ,, ' • -
-0.81
'- • - *"„
-0.23
0.12
-0.23
1.04
-0.35
1.50
''C . '': ->•;"'
0.00
-1.73
-0.58
1.04
0.46
0.00
: ,-*
0.23
0.81
-0.46
•:. " ' , * *
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Strontium-90
Lab
DO
DT
DZ
E
EB
EH
EL
•. V, -.
^ EOS
.." , , .
ER s
EV-'
'EXf
FE
FF,
• FJ '•
,'FL
; FK;.
FU
••\ * ' i"".
1? £t
. GE:;

GI
GQ
G*f
GZ

HH
HI
HK
HL
HP
HU

HX
I
IA
1C
ED
IE
IU
J
JE
JG
JH
JN
JQ
JS
JY
Res. 1
15.0
16.0
13.0
15.0
14.0
14.0
13.0
,. v ^ V ^ ^ «
s"" "" •• s% i ^ ^ ^
"• '
/ •• v"\ ^
- \^
, ^ J \~"
15.0
' ^ -. %s
i , * ' -
^ -^ \»
, '•
12.0
"" *. C w """ ^

\'-N\

* i
12.0


;


14.0

12.0
20.0


18.0
If:
14.0



14.0
14.0




12.0
13.0
Res. 2
17.0
16.0
13.0
13.0
13.0
14.0
14.0
X; ^ f ~l '^'%!i\^\ *
sTf; v\Jv \;fv 5 ^ x
%^,"! V;' \i\C'
14.0
'>yl;-v;?^V
(<5^^;-^,\/f;
\'-7- ^S-Vlt^v:;,'!
* -1* \"- '-'^^X ' ' ' V
13.0
s ----^ *'« * ^ -^\^^
" ^*--\ ^ v' ^\'N '"•
* •• " ''^'-^ •; - '•'"'- •'. " -


12.0
; -;> ' „ '-^,


1 ;- ~ - -~ • * '
- ' * ' f
o" S ' ", -
13.0
- \"\ * sv V.^1.*1
12.0
19.0

' " ' "',- " !>* V*
16.0
^^v;\:*^;
14.0
- x; " ", V' '


14.0
14.0




13.0
15.0
Res. 3
12.0
15.0
14.0
13.0
13.0
12.0
13.0
* TCv •>••
s vv; 0^r,; , ^
"" •. '' :^ "•' 'f- ^

x ;>:^ -
' :'-">V;k,,\
16.0
'^V, T;,"
^-Xi *.'''"S
-i^V-^t
>>^;-H
12.0
, ' -S* ,* \,J.

^ ''- > X

• ' ™v!' - -S
12.0
^vx \,
v™ -*


\ , , s
14.0
~ ','5 '-. • %
10.0
19.0
\v •• s\v

17.0
^>f^:-:
13.0

\

14.0
14.0




14.0
17.0
• = No data submitted
1 0 =
Insufficient
data
x =
Exper.
Rnganal
Sigma (R + SR) Average
2.52
0.58
0.58
1.15
0.58
1.15
0.58
< *


i •. '•: S'V ' * V
;,, ^r jv _ ' ./^
T - % ,x V T" '
1.00
•*- ";\% "^--: ' •
\ s"1 "• ' J " fc '•
\ ^^' : •. s \ "
- " " ,-^V " \
0.58
;, x" s " '

\-\-~ '/; - "


0.00
" -\


- ^-'

0.58
,,•-*"•
1.15
0.58


1.00
vx~ o ,*\ ;,
0.58



0.00
0.00


"••'

1.00
2.00
0.591
0.118
0.118
0.236
0.118
0.236
0.118

N-> •-
s "• *

»'~',Y-.'
• v"'
0.236
r — -:-;
> \11;-1-
^ " " *
--,- ,VJ--:
0.118
", "- *"~ >




0.000

,

~ ; ,

0.118

0.236
0.118


0.236
, '- >'"r> ;:
0.118



0.000
0.000




0.236
0.473
14.67
15.67
13.33
13.67
13.33
13.33
13.33


* C * ^ \v "* X, ^
' x ' ^ ' s -H'\^,- ,>• ;
, f ^":-'! **''.;- '•
,-S-^iIv^'-^
15.00
" ;V:V;i;?-'-v
-•''•'^^r-',';
':.,','- ''^;f^\^^
^(5\^^y
12.33
\ % i V ^ "• ^ ""
'"\-' ""'^ s ,•• ^"^ *^
'^* "\l -X\'^ "^
\ •• "• ^s v

12.00
• ~, ,"'«'c"-' ,i
, '••

' \- x v

13.67
- *-" - - '" ; „ - - ^
11.33
19.33


17.00
,°=' "'* lX ,'v5' ?
13.67



14.00
14.00




13.00
15.00
TAG SYMBOLS
Determined
to be an
outlier
21/50
Normalized deviation
(grand-avg) (known) Tag
0.18 -
0.53
-0.28
-0.16
-0.28
-0.28
-0.28
f ^ •> - ••' •. „•• * ••
- *" \^" ' -- >;\ ^
^ " \ S V ^ ^ * s •> -. """
- --/-"J ;,%-"%- -\ ol^'x
Y^lSt;/£^;Y
V-'vfxF^'^V •:
0.30
*!Kf v.\r1 v
" x1"^ >r,;'- :^-
SV-i^V^>'; s:;
^ f^ •&• '"•'"'• *
-0.62
^r P"VJX' *~"~ ' s^'xv"--8
\ s v , %^^ v'\^^ ^^^ "
, , ,\, v^^.°' 7.^

'-• N v5-; ^-\^% , - ':
-0.74
^^:!r5-/r^.
\ "£' *""~Vvx\,' ^ .\™«"

1 T \?\' "\vV
'C ' s -'•-•• -™' '
-0.16
•- ™^>11« v • • - ,
-0.97
1.80

;;;- '^;;"' \7 f %
0.99
^^Sv?'"""7
-0.16
vv


-0.05
-0.05




-0.39
0.30
ft s Above
li s Below
0.23
0.58
-0.23
-0.12
-0.23
-0.23
-0.23
, • <
' ~'\ - ** •
*~ "' °"", * *
- JV5" . ' •
\* ' ' • ,
••- .! "• • •
0.35
•\~ * y
' , ' . *>
•- vjV^*;-*~
:\ V"> ','«-
-0.58
'•;'•'•• % "• , "• __ -. "• "
\ o "*• +
-,,1 '_-••' ;;{V. -

' • ''; -,'' -•
-0.69
/•-;l>, -.-•
' »

• --
< "-;* -• -
-0.12
* >• * '
-0.92
1.85

- ", -;s \ • "
1.04
«v.- r^?-:*<;
-0.12
•
«
•
0.00
0.00
•
•
•
•
-0.35
0.35
control limit
control limit

-------
227
50
EMSL-LV
Performance Evaluation: Blind-B, 19-Apr-1994
Strontium-90
Lab
K
;KE,
KM
K*f
KX
L
LF
LG
LL
LM
LH
LT
M
MA
MN
MO
MP
MQ
MS
MV
MY
N
NA
NG
NH
Nl/
NJ
NK
NO
NT
O
OF
OS
OX
OY
P
PA
PB
PC
PG
PI
PM
PP
PQ
PR
Res. 1
22.0
, /" '";. ./
14.0
13.0
:\'"' * ''"'''

-'"'. •", ;,

- - - '"";,
15.0
14.0




15.0
V" .:"
14.0

~ ,'•'-, : ':'
1 \ ^ „ f ^ '
• • ' \ ' * '- '
.12.0
11.0"
14.0
v - , t
: - " '"-x


", s


15.0
16.0


13.0
14.0
13.0
Res. 2
2,1.0
/K*%v*?\
15.0
13.0
;,\':;' '' f
* . ' ^ J ' ':'' \
V ' -f" •• ' """•
t '
* " -V-,' ' v;
15.0
15.0
/','/ •"'"'

<- ,'.'•''. '

15.0
i -t ' v V j
14.0
-\'''r'vl ">-'' -' '
o -; V" '^--r"'-',
' ,'^V' ;'- --"?''•-
"\ ' • -" : \x *,
12.0
•.' % \ - " *
11.0
15.0
-.';, /\\'/~"
: - - "],' " "
i 1 •• ••''''•
!v,' * '•-"



15.0
16.0

(
13.0
16.0
11.0
• = No data submitted
0 s
Insufficient
data
Exper.
Res. 3 Sigma ,
18.0 2.08
L'!;. y^i/.A..' -
14.0 0.58
13.0 0.00
• -"^ :• '' ':• " ''J< - •
'',;'•''"•'

',--'• ' - !
; '< , --"'- '
15.0 0.00
14.0 0.58
-


'"''•.^ "" ' , s"^
14.0 0.58

13.0 0.58
'' ' -;/\ ;' \- - , . '
,'* '"..'. ' ::;'',- -/ , ,-
*"•-•"-* '!.-"-,' \ , , -*

11.0 0.58
10.0 0.58
15.0 0.58
, !f"'; V ';;',, -'
".-*.'. t '. - ;/ ;
"'- ' --' V_ ,
' . ' ; : ', v - ''s


,
15.0 0.00
17.0 0.58
<

v 13.0 0.00
17.0 1.53
14.0 1.53
' %}' "•• v. "* ^ "" ' %
Rng anal
(R + SR)
0.473
v „ ' , •'
0.118
0.000





0.000
0.118




0.118

0.118




0.118
0.118
0.118







0.000
.0.118


0.000
0.354
0.354
Average
20.33
'i '-
14.33
13.00
- i •''
-;



15.00
14.33




14.67

>
13.67



7
11.67

10.67
14.67

-. y





15.00
16.33


13.00
15.67
12.67
TAG SYMBOLS
x = Determined
to be an outlier
Normalized deviation
(grand-avg) (known) Tag
2.15
I ,\ *,',•• !- ' 'V/J1'
0.07
-0.39
', '/ V;; ;_; •','""
/--, • >: - -
v ^ '
' ' "^ •• ••

0.30
0.07
•-h

f\ *
^ " ''"'"
0.18
-,,;.Y:.r;-^
- \ - > -. ^/
-0.16
.' -, :, . '-,:''' "-"',,
'<••• ' >'*' ,:-' f'~-
: s, '• - - * '1 , * ; " '
"'-"'"-. ,- '-;• •
-0.85
", ' ' „ -' >":'-:
-1.20
0.18
{,':',--', , ' ',
"';;, -";-' ^ ;';<
-- '"' ' * ' V* ,' •
\ " \ "

x

0.30
0.76
*•

-0.39
0.53
-0.51
ft H Above
^ = Below
2.19
•i- -;"' '-',^1' ':*•'<
0.12
-0.35
''•'- ":-; ' -'-•;'-
^ - ••' -. -••
" " s >v '*" -
~>/^'^~
..'•; -- • '
;' ".\»V
0.35
0.12
j= ; -' ' ^ •„ '
-/•"<,-'. •' »^«,
/>>v: ^-'~-
' - , '',,•'
0.23
^ t s' ^ ' -."" '''••
J, ""t :?Z * * j"'i' "• /"'1,
'',"''> V , * ' '
-0.12
}V'?\:'f -''„•-,;,
v, ^,^
///>';;';'i'»; \
- , 1 ','•*''
-0.81
;/,V -vv-"*'
-1.15
0.23
- -V/ ; vi-^\
; X- f v * •• i'f
<-s '
" tf Jj *, "
"-" ;-/!-'-.",»f-'.
*
' •
• .
0.35
0.81
• '
- ,»
-0.35
0.58
-0.46
V.,;' " •' f
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
23 / 50
Strontium-90
Lab
PT
PV
PW
PY
Q
QC!
QJ
QK
QL
QP
QQ
,QT
QU
QW
CF5T '
. T^A.
QY
QZ
RC
RD
RE
RF
RG
RJ
RK
RL
RM
RP
RR
RV
RZ
S
sc
SD
SI
SL
SM
SO
SR
ss
ST
SW
SX
sz
T
• =
0 3
Res. 1
6.0
13.0
'

16.0

13.0
14.0
12.0
. C "* **
:• J*:: '>':
2s;o
14.0
. % ^ " ," ^ v
""X\
M
13.0
14.0

>





15.0

14.0
20.0
••:^v."
16.0
14.0
15.0
V5
18.0

9.0


14.0
13.0
10.0

18.0
13.0
Res. 2
7.0
11.0
-s
, *
15.0
*s .\ ^
13.0
14.0
12.0
ip'F^vJ;'
•3t ₯'f'
\^:!24o,%
16.0
••""s ^\ , S S '
\ " '?* ^^
X^v
12.0
12.0





"
xt s
16.0
-•
14.0
18.0
-
15.0
12.0
14.0
18.0
, '. ' Y;::.
11.0


15.0
12.0
11.0
••; -V-\' :< .k.;,vk
15.0
13.0
Res. 3
7.0
10.0


18.0

14.0
15.0
10.0
; ^ •• ^ x -•"'• j:'1'1 «••''''
S::|S-
*?; '\27,o^:
18.0
«s "" *• "
^ " sl ^ ^%"1-'' %-.-•! ^
\ """ '
13.0
11.0




' <
•-
\
16.0
^
15.0
18.0
>-
16.0
13.0
14.0
19.0

9.0


15.0
13.0
12.0
;.-..-. :<|<.'-^
17.0
13.0
No data submitted
Insufficient
data
x =
Exper. Rng anal
Sigma (R + SR) Average
0.58
1.53
v

1.53
-
0.58
0.58
1.15
-. \\ -. -.H '•'•''''•
\ *^ i % ••
: 2.08;
2.00



0.58
1.53
v <
f



-

0.58

0.58
1.15

0.58
1.00
0.58
0.58

1.15


0.58
0.58
1.00
•',->' • • • • • • •
1.53
0.00
0.118
0.354
N
--
0.354
-
0.118
0.118
0.236

v r^V-
0.473
0.473

W " v-- "
' -" :
0.118
0.354







0.118

0.118
0.236
-
0.118
0.236
0.118
0.118

0.236


0.118
0.118
0.236

0.354
0.000
6.67
11.33
\ V
h
16.33

13.33
14.33
11.33
/ol/r, ix~ ;>="-, -xC
>:.°H^ Cv> ^"
-':-^A\26^3-^
16.00
s " -. J •- " ' ""^
*'"• ' ; ; ^ ^ "• ^ ^ V0
. ',;.>^rvivV^;
12.67
12.33
f

>
^

-
•=
15.67
' \ > *
14.33
18.67
•t *•
15.67
13.00
14.33
18.33
.-•.''•••'• " '•. -c,,t:
9.67


14.67
12.67
11.00
v
16.67
13.00
TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known) Tag
-2.59
-0.97
"{ \-- \
,-
0.76
< <
-0.28
0.07
-0.97
^s^r^-':^
:;r^\^jip
-;';>^4i23C-^-
0.65
"" s «o ""? i-0'""''
*t "" •- 1 * "• ^ -.\ , •• "s "

-0.51
-0.62
"*s -^ x?
>
s -5
! x '\
11 ^
"• " > ^ ^
r x **
0.53
<
0.07
1.57 ^
\ AX \
0.53
-0.39
0.07
1.45

-1.55


0.18
-0.51
-1.09
' •, >
0.88
-0.39
IT 3 Above
li = Below
-2.54
-0.92
* \
«
0.81
Xs •
-0.23
0.12
-0.92
- "; •'•-*
,;---; , ,,s/-
4.27 x
0.69
» V "
J s V ^ ' ^ "
N • - ,- . ' «
-0.46
-0.58
*
1 •
•
•
«
V-' *
•
0.58
v .. •
0.12
1.62
.*
0.58
-0.35
0.12
1.50
«:•:,
-1.50
• .'" : * •'•
"-V,:. ••..'•
0.23
-0.46
-1.04
' •- - • ./
0.92
-0.35
control limit
control limit

-------
r
24/50 EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Strontium-90

Exper. Rng anal
Lab Res. 1 Res. 2 Res. 3 Sigma (R + SR)
TA • •"•' -.v:.»,;-- ' :' <
> ••' v1" - X %* s •-" ' "'' ',,'.,
UE 14.0 15.0 16.0 1.00 0.236
VG r:~ ••-•-; - ;: :' * •-',/- -
UK - •' •• , "\ '" .;
UN< ' - ' ' •
-^-"' J- -' s *" * 1 ' / / ' s
UP 13.0 16.0 17.0 2.08 0.473
UQ -' ../ •'• - - . -

UW 14.0 14.0 14.0 0.00 0.000
UY '-' ' •»'"„••'"' -
VA • , - , ' ' '
vc ': '- •• "'•/•;> ;. . ' •'•'
^ x ' ' ^ '

v- , - - -•.- .- .;•-,- ', • !-
VG 13.0 12.0 13.0 0.58 0.118
vi ...''-.' •• :" / .
VJ ,.X- ' .;•>•,-"
;VM ' - , ' ,_ x./
VO-" > ' , :'°- '"'' - : :'/'"
'VQ '" V . „ ,
VT • •-:-.- ^>,- • ^"^

\' •;' "•" '- " ••-' • ' ~ '

- ,- . . -•
' - ^ ^ ^ '
'AT -7'- ''. -,'-'/ ;-'- '-, ' _,-
W 14.0 14.0 13.0 0.58 0.118
WA • ' -',..,•:••

X 9.0 11.0 11.0 1.15 0.236
Z 14.0 14.0 14.0 0.00 0.000

Normalized deviation
Average (grand-avg) (known) Tag
- '-/'•'••"/'•'; ' -'4-V"!'.Vi -'"-:•„'
12.00 -0.74 -0.69
18.67 1.57 1.62
• ' • - %- :- - ,; ' ; -••'
- - .,'." '* \' ,y^-v- •-•  ** ">* ' •
14.67 0.18 0.23
14.33 0.07 0.12
V '-.... "r ;'...'< *.,'j.... -';.;.' JV'C '' ; V %r ' -
15.33 0.42 0.46
- , ,;,. -V" ; -V- :^r, ,:^;^r»-"r ,-""
15.00 0.30 0.35
:;.:. \>;"'-' ///."vXH^Vl*^
-" ' - • '•"">''''-' '"•-•„
15.33 0.42 ,,0.46
. -•' - j' • /" "V '
14.00 -0.05 0.00
'" ,' ^ - "; V- />i ''><>--,.:>• */'
-•.-'• --:- - .-• .' • • ,<''' v X.?- ,
'; '• ', / '- ' • - ;_ ; ' • ,^''< !,^-> - - •-*. --
12.67 -0.51 -0.46
- •',' V ,::,-, \»f
' ^v':':- - '•/",- '';"*'''": "-':%''>x >;*-.•.-'
^; ' •"-• ::;; - •' '.: *; '
" . X-'V': X vy^v: v:H-;K
:- - • '"- ,lV-, '- ""7*^''
-'<•-" ''•--, ' „' !'-!V-1--y \;>;: • '
13.67 -0.16 -0.12
• " '- > ' ' ' , s -•. ; ,». -•
10.33 -1.32 -1.27
14.00 -0.05 0.00
Data sorted by Laboratory Average
Average Tag Lab
6.67 PT
9.00 CP
9.67 SM
10.33 X
10.67 NO
11.00 SW
• = No data submitted
0 = Insufficient data
Average Tag
11.33
11.33
11.33
11.67
11.67
12.00
TAG SYMBOLS
Lab Average Tag Lab
QL 12.00 GQ
PV 12.00 BG
HP 12.00 AE
NJ 12.33 RC
BO 12.33 FU
TD 12.33 CQ
ft = Above control limit
x s Determined to be an outlier & = Below control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Strontium-90


25/50
,
Data sorted by Laboratory Average
Average Tag
12.67
12.67
12.67
12.67
12.67
13.00

13.00
13.00
13.00
13.00
13.00
13.33
13.33
13.33
13.33
13.33
13.33
13.33
13.33
13.67
13.67
13.67
13.67
13.67
13.67
13.67
14.00
14.00

% responding labs
Lab
VG
ST
QZ
PQ
DG
T

SC
PM
L
JS
CJ
QJ
EL
EH
EB
DZ
CE
C
AF
W
N
1C
HK
E
AA
A
Z
UW

Average Tag
14.00
14.00
14.00
14.00
14.00
14.00
A
14.00
14.33
14.33
14.33
14.33
14.33
14.33
14.33
14.33
14.33
14.67
14.67
14.67
14.67
14.67
14.67
14.67
15.00
15.00
15.00
15.00
15.00

Frequency distribution
Lab
JE
J
D
CO
BL
BC

AZ
TS
TL
SD
RR
QK
M
KX
CA
BA
TQ
SS
NT
MQ
DO
DD
AU
UE
TI
PB
LT
JY

Average Tag
15.00
15.00
15.00
15.33
15.33
15.33

15.67
15.67
15.67
15.67
16.00
16.00
16.00
16.00
16.33
16.33
16.33
16.67
17.00
17.00
17.00
17.67
18.33
18.33
18.67
18.67
19.33
20.33
26.33 x

Lab
FE
BH
AL
UP
U
CX

S
RM
PP
DT
QW
BM
AK
AJ
Q
PC
DE
SZ
I
CS
CG
AW
SI
CK
TE
RV
HU
K
QU



10

-6 -4
IUllli-
Illlllll-
-2 ' I T

1. -
+2 +4


I i
Normalized deviation of the mean from the known value
• 3 No data submitted
0 3 Insufficient data
TAG SYMBOLS ft a Above
x = Determined to be an outlier li = Below
control limit
control limit

-------
26 / 50          EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994

Strontium-90

 % responding labs	Frequency distribution
 10-
     -6            -4            -2             0            +2           +4           +6
                    Normalized deviation of the mean from the grand average

-------
                  EMSL-LV Performance Evaluation:  Blind-B, 19-Apr-1994
                                   27/50
CobaIt-60                           Statistical Summary                       216 Participants

The known value of this nuclide is 20.0 pCi/1 with an expected precision of 5.0; the control limits
are 11.3 to 28.7; the warning regions are 11.3 to 14.2 and 25.8 to 28.7
7O(32.4 %) Failed to respond .
4(1.9%) Outliers '


         Statistic
               ; 140(64.8 %) Within all limits


Respondents
- 2(O.9 %) In warning zone

         but within control
      .


            Non-outliers
Mean
Std. Dev.
Variance

%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
20.12
2.60
6.75

12.92
0.59
0.05
20.00
0.00
0.00
Grand Avg 20.12
1.83
3.35

9.10
0.60
0.07
20.00
0.00
0.00
4(2.7 %) More than 3 norm. S.D. «.%
           . 128(87.7 %) Within 1 norm. S.D.
                           of known value
2(1.4 %) Between 2 and 3 norm. S.D. •

     '• 12(8.2 %) Between 1 and 2 norm. S.D.

-------
28 /
50
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
Cobalt-60
Lab
A
AA
AE
AF
AI
AJ
AK
AL
AO
AP
AE
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
IBS '
BW
C
CA
CE
ca
CJ
CK
CM
CO
CP
CQ
CS
CX
D
ID!';
DD
DE
DG
DI
DL
DM
• =
10"
Res. 1
21.0
19.0
19.0
22.0
20.0
23.0
19.0
29.0

19.0

24.0
16.0
20.0
21.0
19.0
27.0
22.0
20.0
20.0
20.0
18.0
20.0

18.0
20.0
20.0
18.0

25.0
21.0
21.0
21.0
20.0
23.0
21.0
21.0
20.0
'... ..::. . :, :• . .
18.0
20.0
22.0

20.0
20.0
Res. 2 Res. 3
21.0
20.0
22.0
19.0
20.0
25.0
19.0
25.0
\ '',; .*;/ ' _
21.0
/
23.0
18.0
19.0
21.0
19.0
22.0
22.0
19.0
20.0
22.0
20.0
23.0

18.0
19.0
20.0
18.0
' ;v '
26.0
23.0
19.0
19.0
20.0
22.0
22.0
22.0
19.0

18.0
20.0
21.0
+ •>
20.0
21.0
21.0
19.0
23.0
19.0
19.0
23.0
19.0
23.0

21.0

19.0
16.0
18.0
24.0
18.0
26.0
18.0
20.0
20.0
21.0
20.0
19.0

5.0 ,
19.0
21.0
22.0

20.0
22.0
26.0
24.0
21.0
23.0
22.0
20.0
20.0

19.0
20.0
21.0

20.0
22.0
No data submitted
Insufficient
data
x =
Exper.
Sigma
0.00
0.58
2,08
1.73
0.58
1.15
, 0.00
3.06
--.;>--- -
1.15

2.65
1.15
1.00
1.73
0.58
2.65
2.31
0.58
0.00
1.00
1.15
2.08

7.51
0.58
0.58
2.31

3.21
1.00
3.61
2.52
0.58
0.58
0.58
1.00
0.58

0.58
0.00
0.58

0.00
1.00
Rnganal
(R + SR) Average
0.000
0.118
0.473
0.354
0.118
0.236
0.000
0.709

0.236

0.591
0.236
0.236
0.354
0.118
0.591
0.473
0.118
0.000
0.236
0.236
0.473

2.020
0.118
0.118
0.473
*
0.709
0.236
0.827
0.591
0.118
0.118
0.118
0.236
0.118

0.118
0.000
0.118

0.000
0.236
21.00
19.33
21.33
20.00
19.67
23.67
19.00
25.67
':. * ',
20.33

22.00
16.67
19.00
22.00
18.67
25.00
20.67
19.67
20.00
21.00
19.33
20.67
> " '"
13.67
19.33
20.33
19.33
• ' -
23.67
22.00
22.00
21.33
20.33
22.67
21.67
21.00
19.67

18.33
20.00
21.33

20.00
21.00
TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known) Tag
0.30
-0.27
0.42
-0.04
-0.16
1.23
-0.39
1.92
- ^ -- > '
0.07

0.65
-1.20
-0.39
0.65
-0.50
1.69
0.19
-0.16
-0.04
0.30 '
-0.27
0.19
, '- >-,'>'
-2.24
-0.27
0.07
-0.27

1.23
0.65
0.65
0.42
0.07
0.88
0.54
0.30
-0.16

-0.62
-0.04
0.42

-0.04
0.30
ft = Above
U = Below
0.35
-0.23 :
0.46
0.00
-0.12
1.27
-0.35
1.96
^ , ,. • ,
0.12
*
0.69
-1.15
-0.35
0.69
-0.46
1.73
0.23
-0.12
0.00
0.35
-0.23
0.23
'•;T > - ~.\ - #
-2.19
-0.23
0.12
-0.23
- "'; ;-/."
1.27
0.69
0.69
0.46
0.12
0.92
0.58
0.35
-0.12
, ' .
-0.58
0.00
0.46
, • .
0.00
0.35
control limit
control limit

-------

EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
29/50
f Cobalt-60
Lab
DO
DS
DT
DZ
E
EB
EH
EL
EO

EV
VEX-'
FE
FF-
FJ
FL
'FN-
FU
FZ
GE
GI
GQ
GT
GZ
HH
HI
HK
HL
HP
HU
HX
I
IA
1C
n>
IE
IU
J
JE
JG
JH
JN
JQ
JS
JY
Res. 1
20.0

22.0
18.0
21.0
19.0
18.0
19.0
- :X- ™ x .-
•^X ^ - ^ ""
•^ ••>
V" ' ~ >C
21.0
:'-v!-;'^
22.0
20.0
21.0
24.0
20.0
19.0
20.0



36.0 -.!
20.0
19.0
21.0
17.0
22.0
17.0
21.0



20.0
20.0
18.0



19.0
23.0
Res. 2
23.0

19.0
17.0
20.0
19.0
20.0
20.0
Jtliij
vj\ ^^ ^ \ •. "
\ ' V -*vf ,v
'^vi'vf*^
18.0
ve^r^r
23.0
21.0
21.0
23.0
20.0
20.0
20.0

>f ' /
s ••ry'x
^3lX)'v
20.0
21.0
22.0
17.0
20.0
20.0
20.0



19.0
20.0
16.0



19.0
20.0
Res. 3
19.0

21.0
18.0
21.0
19.0
20.0
18.0
^fi=\iv';^;
vX*- ;w^"\"-' N '""^x"'"''1
,^; s-V^-t :' \
;s!^x'{^f;V;,\,
15.0
vp;, -;"-:, ];;.;-;
21.0
21.0
18.0
24.0
20.0
19.0
20.0
% s ^ "^^i-.
\ ,?
5 : , '> ' '/'•" ,v°
;'>-- - 27;0^'
20.0
22.0
22.0
16.0
23.0
18.0
20.0



19.0
21.0
22.0



20.0
23.0
• = No data submitted
[ 0 =
Insufficient
data
x =
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
2.08

1.53
0.58
0.58
0.00
1.15
1.00
x s " -- --' -^-o%-, *0*v
>•• ""^ \ -.'^ %\ "tw \> " ^^
;<" ,' ,",,'V' '\, -
s • %'*\*1'
3.00
= ' - '- ! ""'• ~. '
1.00
0.58
1.73
0.58
0.00
0.58
0.00



-t-« \4i5l\~- '«>
0.00
1.53
0.58
0.58
1.53
1.53
0.58



0.58
0.58
3.06



0.58
1.73
0.473

0.354
0.118
0.118
0.000
0.236
0.236
i V:;
x% -
-/,
=V \ '
0.709
-v-
0.236
0.118
0.354
0.118
0.000
0.118
0.000
\ •• ,

/;>
1.120
0.000
0.354
0.118
0.118
0.354
0.354
0.118



0.118
0.118
0.709



0.118
0.354
20.67
, -
20.67
17.67
20.67
19.00
19.33
19.00
•";> &fr>'^?v
*^* ••»-:\'-^\ \\^ v"-- >^">^ **V-*
,-••-•. -- "' '" ^i'^"< - ;
\:^; -,,-^'> "v ->
18.00
- - >* V' ------"> s \-
22.00
20.67
20.00
23.67
20.00
19.33
20.00


\ \XV";'' '-""' ",'!>
,". >;^i.38^":
20.00
20.67
21.67
16.67
21.67
18.33
20.33



19.33
20.33
18.67



19.33
22.00
TAG SYMBOLS
Determined to
be an
outlier
0.19
N
0.19
-0.85
0.19
-0.39
-0.27
-0.39
V^'^V^^V""
"\ ^-." % ^S\^sx^ ^ '
x"-^. ,-'""• •_,_ ^ ,v •
•C^x"*";'"-'- *
J3.73_
Sv^'^'^ v ,
0.65
0.19
>•-
-0.04
1.23
-0.04
-0.27
-0.04
' v^ s % -• T -f, ^
\ s^ ^V1-'1- "" i
•.s ^ ?v '"'"•.^
>^v^^"
,^;^8|IV:,:
-0.04
0.19
0.54
0.54
-0.62
0.07



-0.27
0.07
-0.50
N


-0.27
0.65
IT s Above
& = Below
0.23
\
0.23
-0.81
0.23
-0.35
-0.23
-0.35
s, s ^"''''-T*' vv
'- ^ s % ""\ •" - , ,
, '<.' "' - \ • * *
\->'-° • \«:'v
-0.69
»-> - •*
0.69
0.23
0.00
1.27
0.00
-0.23
0.00
• ' '- v *
• x^: = V* '
\;v--!;^\,"^ - •--•
%93: -x
0.00
0.23
0.58
-1.15
0.58
-0.58
0.12
•
«
•
-0.23
0.12
-0.46
' •'•
' .••'
' • '
-0.23
0.69
control limit
control limit

-------
30 /
50
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994

Cobalt-60
Lab
K
' KE
KM
KT
KX
L
LF
LG
LL
LM
LR
LT
M
MA
: MN
MO
MP
MQ
MS
MV
MY
N
NA
•NG'
NH
NI
NJ
NK
NO
NT
O
OF
OS
OX
OY
P
PA
PB
PC
SPG
PI
PM
PP
PQ
PR
• =
0 s
Res. 1
22.0

19.0
21.0
20.0
21.0


i
20.0
20.0
19.0
23.0
- v-' ' ' ,\
',
14.0
22.0
22.0

22.0


20.0

19.0
19.0
15.0
21.0
• ' > • ! -
, -, ,
31.0

20.0
22.0
•f
19.0
23.0
20.0
20.0
< < "•
Res. 2 Res. 3
23.0
, '
22.0
20.0
20.0
22.0
,, >-\ '*\\'


19.0
20.0
18.0
23.0

i
17.0
25.0
21.0
" " " f
20.0

•*J } ''; '
21.0
- - , , " *•
19.0
18.0
15.0
21.0
,.-'"' ! , .

32.0

20.0
23.0

19.0
21.0
24.0
19.0

24.0

19.0.
23.0
20.0
18.0

' """s s? .. ' .- '

22.0
20.0
18.0
22.0
^

17.0
21.0
22.0
--
22.0

I'
19.0
"• *
19.0
20.0
15.0
21.0
-•^


31.0

20.0
24.0

19.0
21.0
23.0
20.0

No data submitted
Insufficient
data
x =
Exper.
Sigma
1.00

1.73
1.53
0.00
2.08

-V*
0.58

0.00
1.00

0.00
1.15
2.08
0.58
•-,
Rng anal
(R + SR) Average
0.236

0.354
0.354
0.000
0.473



0.354
0.000
0.118
0.118


0.354
0.473
0.118

0.236


0.236

0.000
0.236
0.000
0.000

> ; -
0.118

0.000
0.236

0.000
0.236
0.473
0.118

23.00

20.00
21.33
20.00
20.33
,. , * " -• ' S •• s^
-" - -
,Y % ; .
20.33
20.00
18.33
22.67
• /"•'

16:00
22.67
21.67
' * ' '
'21.33


20.00

19.00
19.00
15.00
21.00
, .-?
"" ••-
31.33

20.00
23.00

19.00
21.67
22.33
19.67

TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known) Tag
1.00

-0.04
0.42
-0.04
0.07
-f, ./ > :; 7'"'1 "
- , "•"- •' -

0.07
-0.04
-0.62
0.88
•>' -;'',' ' '' ",• ,,

-1.43
0.88
s \
0.54
Y" - ;'->''- ;- :x
0.42

'• , s ^ '
-0.04

-0.39
-0.39
-1.77
0.30
f * ••
; '- , ", «, ,"'
3,88

-0.04
1.00

-0.39
0.54
0.77
-0.16

ft = Above
U = Below
1.04
^'r'','*'», ','•'.'*
0.00
0.46
0.00
0.12
''' "''" " ,* '
\;; \ «,;
= ••
0.12
0.00
-0.58
0.92
,"'y V\ '', »;\,
' *
-1.39
0.92
' '," ,'* '
0.58
•6. *
0.46
^ ./ •
"-.V''f' - >
0.00
, " / " . •
-0.35
-0.35
-1.73
0.35
^:/rcv! \;*
'' •' ' ' '' * '
3.93 x
•
0.00
1.04
, * '•
-0.35
0.58
0.81
-0.12
' -' > :<•'
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Cobalt-60
Lab
PT
PV
PW

PY
Q
QC
QJ
QK
QL
QP
oo
*c*t
QT
QU
QW
QX
QY
QZ
RC

RD
RE

RF
RG
RJ

RK
RL
RM

JCVJr
RR
RV
RZ
S
sc
SD
SF
SI
SL
SM
SO
SR
ss
ST
SW
sx
sz
T
Res. 1
:'....• 49.0. ••
23.0
20.0


18.0
*
20.0
20.0
19.0
19.0

20.0
19.0
19.0
25.0
- V
19.0
18.0




"' 9iO \
\ \s .'
o- --

'-> x •'
. - ~ ' •• x>
17.0

19.0
20.0
18.0
21.0
20.0
22.0
20.0
20.0

19.0

23.0
19.0
19.0
19.0
17.0
20.0
19.0
Res. 2
'*'."• -9.0-;. ;
20.0
21.0

.- "\X'x".
19.0
s ' ^ N \«. -.
20.0
20.0
19.0
22.0
,~ >\ ' ,^ ' ^ « ° -~
19.0
17.0
19.0
26.0
*x
19.0
18.0

,._••'•...•>'• .--^A ' •• •• ••
, ^ ^ ; t ^ ^

; 6.0 ^
*::•• "^:'\:\^y
'" ,..-,, -I ^\ -K>

«\ •' - \~- »*^,x
1 v*~ s •- " ""^ s\
19.0
"; '• "' " ! ,
20.0
16.0
20.0
21.0
19.0
15.0
20.0
21.0

19.0
,
20.0
20.0
19.0
19.0
17.0
20.0
18.0
Res. 3
9,0
25.0
20.0


20.0
"\V ! i«^, o
23.0
20.0
19.0
26.0
~ \i - •.*"
18.0
18.0
24.0
240

18.0
19.0

: Xv-™i-x>
^ v"1 ^ -. ^

Q f\
- _ , -s\^;- :
; ;> '%s

. VX>",*r^' •'
• ^ *••? ^ ^ v
19.0 ,
• ' ,<." '-
23.0
20.0
20.0
21.0
19.0
22.0
19.0
21.0

20.0
•|' ' :::'! ' ' •
21.0
17.0
19.0
18.0
25.0
20.0
18.0
• = No data submitted
10 s
Insufficient
data
x =
Exper. Rng anal
Sigma (R + SR) Average
0.00 ;
2.52
0.58


1.00
^ \\v~V ,-,, -
1.73
0.00
0.00
3.51

1.00
1.00
2.89
1.00

0.58
0.58

-/<


•" '0.58'",
,.-" '*'-~v ~


* ^

1.15

2.08
2.31
1.15
0.00
0.58
4.04
0.58
0.58

0.58
H*
1.53
1.53
0.00
0.58
4.62
0.00
0.58
0.000; -v
0.591
0.118


0.236
, V, "-,\ ;<.••;,{
0.354
0.000
0.000
0.827
•,/>
0.236
0.236
0.591
0.236
,
0.118
0.118

\ - ,» -" «'
--> ' ,•-, -,

0.118: :\f
^\ --;• ^ ' " " >"
s "" \ V >. "• '

x *-. '

0.236

0.473
0.473
0.236
0.000
0.118
0.827
0.118
0.118

0.118

0.354
0.354
0.000
0.118
0.945
0.000
0.118
9.00
22.67
20.33


19.00
4*v.-*«
21.00
20.00
19.00
22.33

19.00
18.00
20.67
25.00
-
18.67
18.33

^ V - \"
, -. " %1;\ "• "

;-8:674
~ v- •' -
, * '"' ,' \-
^ ^ \ *
- '."r ;j,^
:-^ '->,<'
18.33
, . - V -J-- ™,
20.67
18.67
19.33
21.00
19.33
19.67
19.67
20.67

19.33

21.33
18.67
19.00
18.67
19.67
20.00
18.33
TAG SYMBOLS
Determined to
be an outlier

31/50
Normalized deviation
(grand-avg) (known) Tag
!x^&85x:;,;
0.88
0.07

-"-' ,\'-'--' \ A-1
-0.39
/ \ v^\ T~ %/ ^r
\j^ ''"•"**• --~s -'.;"••.'" •
0.30
-0.04
-0.39
0.77
,,- " i '• *v k . -
-0.39
-0.73
0.19
1.69
' ^ s -
-0.50
-0.62

, x- s*V -Vv--" "v- '.v'.'
of 'f'-^v;,^, \ V\'*

,"};;. --3,97 ^7fr
--- ";- /^OA^V ; T"
^/*^^A'/-X;

"- "- "C^s ••''^ ,:i '
: J"-; ' ,'vx'.f0';.x
-0.62
j \ ,"f vr' x1 ^ ~' '•
0.19
-0.50
-0.27
0.30
-0.27
-0.16
-0.16
0.19

-0.27

0.42
-0.50
-0.39
-0.50
-0.16
-0.04
-0.62
ft = Above
$ = Below
-&81 x
.0.92
0.12
. ^ •. ^
-'•^ -•",-.,•
-0.35
-V; vO • V
0.35
0.00
-0.35
0.81
<•
-0.35
-0.69
0.23
1.73
• \
-0.46
-0.58

- "Vt.^ ; V*- ,
;,-,*,.,,, \x -v0i .

-3.93 x
'''-'; :\ "V'« '
- v" "' • > V «x --'

,-x. ,'>r;y ,-N
•
-0.58
; °
0.23
-0.46
-0.23
0.35
-0.23
-0.12
-0.12
0.23
............ .... ^ ......
-0.23
j.,-. ':''. - • ,,
0.46
-0.46
-0.35
-0.46
-0.12
0.00
-0.58
control limit
control limit

-------
32/50
EMSL-LV Performance Evaluation: Blind-B,
19-Apr-1994
Tcobalt-60
Lab
TA
TD
TE
TH
TI
TL
TN« ''
TQ
TS
TU
TO "'
U
UA
UE
UG
UK
UN
UP
UQ
uw
UY
YA
. YC —
VI
VJ
VM
VN
vo
VQ
VT
W
WA
X
Z
Res. 1
14.0
20.0
19.0
21.0
23.0
18.0

18.0
18.0
18.0

21.0

21.0
*f

19.0
16.0

20.0
20.0

19.0
20.0
17.0
18.0
19.0
21.0
20.0
Res. 2
14.0
21.0
20.0
22.0
22.0
18.0
* "* "•"''•."
20.0
20.0
19.0
, " - - X 5
21.0

21.0
*; ,t '/' \

21.0
18.0
/-';'• ,' ''.-•• -
20.0
17.0
;:,.:;;|;
19.0
19.0
20.0
18.0
19.0
21.0
20.0
Res. 3
14.0
22.0
19.0
21.0
23.0
29.0


19.0
19.0
18.0


21.0


21.0

- ' - -


21.0
19.0

» -
17.0
19.0
f

20.0
24.0
23.0
17.0
19.0
21.0
18.0
Data
Average
8.67
9.00
13.67
14.00
15.00
16.00







Tag
X
X




Lab
RF
PT
BW
TA
NO
MP
Exper.
Sigma
0.00
1.00
0.58
0.58
0.58
6.35
• x>'' *; \ y.
1.00
1.00
0.58

0.00
,
0.00


1.15
1.53

1.73
1.53

0.58

2.65
3.00
0.58
0.00
0.00
1.15
Rnganal
(R + SR)
0.000
0.236
0.118
0.118
0.118
1.570
c -•>
0.236
0.236
0.118

0.000

0.000


0.236
0.354

0.354
0.354

0.118

0.591
0.709
0.118
0.000
0.000
0.236
Average
Normalized
(grand-avg)
14.00
21.00
19.33
21.33
22.67
21.67
-~ r 5,


19.00
19.00
18.33



21.00



21.00





* '
20.33
17.67

-..>;,;
\~-r--
19.00
18.67


-. j ,
19.33
21.00
20.00
17.67
19.00
21.00
19.33
-2.12
0.30
-0.27
0.42
0.88
0.54
\ ' , ',
-0.39
-0.39
-0.62
.-,;/-•.
0.30
^ i * "" ^
0.30
\ ' '

0.07
-0.85
\- - - - :';-
0.39
-0.50
, '" • -' '
1 ">> \ l •. '
-0.27
-,< -, , ,
0.30

-0.04
-0.85
-0.39
0.30
-0.27
deviation ,
(known) Tag
-2.08
0.35
-0.23
0.46
0.92
0.58
•;^, : V-7"^' v
-0.35
-0.35
-0.58
. \:"?.'v S7V»
0.35
' ^ '<*<;/ {' * '.-
0.35
/,'•• ',:-:'--*',
, -, ,, ,: ^; ,,^
0.12
-0.81
>:\. •- Vx :':••-
-0.35
-0.46
•''x'''^'\l ''-•?-
>/cf;"-K-, --•- '•
-0.23
/ ,' ' *
','• '": ' s \ * •"'
'*' ." ' *
0.35
\ % -••• "" *]
0.00
-0.81
-0.35
0.35
-0.23
sorted by Laboratory Average
Average






• = No data submitted
0 = Insufficient data
X
16.67
16.67
17.67
17.67
17.67
18.00
Tag






Lab
HU
AW
W
UP
DZ
QU
Average






18.00
18.33
18.33
18.33
18.33
18.33
TAG SYMBOLS
= Determined to be an outlier
Tag Lab






FE
TU
T
RM
RC
M
It = Above control limit
U = Below control limit

-------
EMSL-LV Performance
Cobalt-60

Average Tag
18.33
18.33
18.67
18.67
18.67
18.67
18.67
18.67
18.67
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.00
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.67
19.67
19.67
19.67

• = No data submitted
10 = Insufficient data

Data sorted
Lab
IA
DD
UY
SW
ss
RV
QZ
JG
BC
WA
UW
TS
TQ
ST
QT
QL
Q
PI
NK
NJ
EL
EB
AZ
AK
Z
VG
TE
SM
sc
RZ
JS
J
GI
EH
CE
C
BN
AA
sx
SF
SD
PQ

Average
19.67
19.67
19.67
20.00
20.00
20.00
20.00
20.00
20.00
20.00
20.00
20.00
20.00
20.00
1 20.00
20.00
20.00
20.00
20.00
20.33
20.33
20.33
20.33
20.33
20.33
20.33
20.33
20.33
20.67
20.67
20.67
20.67
20.67
20.67
20.67
20.67
20.67
20.67
21.00
21.00
21.00
21.00
21.00
Evaluation: Blind-B, 19- Apr- 1994

by Laboratory Average
Tag Lab
D
BK
AI
VT
SZ
QK
PB
NH
LT
L
KM
HK
GQ
GE
FU
DL
DE
BL
AF
UN
PW
LR
LF
JE
1C
CP
CA
AP
SI
RR
QW
HL
FL
E
DT
DO
BO
BH
X
vo
UE
U
TD
Average
21.00
21.00
21.00
21.00
21.00
21.00
21.00
21.33
21.33
21.33
21.33
21.33
21.33
21.33
21.67
21.67
21.67
21.67
21.67
21.67
22.00
22.00
22.00
22.00
22.00
22.00
22.33
22.33
22.67
22.67
22.67
22.67
22.67
23.00
23.00
23.67
23.67
23.67
25.00
25.00
25.67
31.33
31.33
TAG SYMBOLS ft =
x = Determined to be an outlier 11 =
33 / 50


Tag Lab
S
QJ
o
DM
CX
BM
A
TH
SR
N
KX
DG
CO
AE
TL
PM
MV
I
HP
CS
JY
FJ
CM
CK
BA
AU
QP
PP
TI
PV
MQ
MA
CQ
PC
K
FZ
CJ
AJ
QX
BG
AL
x P
x HI
Above control limit
Below control limit

-------
34/50          EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994

Cobalt-60

 % responding labs	Frequency distribution	
 10
     -6            -4            -2            0            +2  '          +4            +6
                     Normalized deviation of the mean from the known value
   responding labs	Frequency distribution
 10-
     -6            -4            -2            0            +2            +4            +6
                     Normalized deviation of the mean from the grand average

-------
                 EMSL-LV Performance Evaluation:  Blind-B, 19-Apr-1994
                                                 35/50
Ceaium-134
Statistical Summary
       216 Participants
The known value of this nuclide is 34.0 pCi/1 with an expected precision of 5.0; the control limits
are 25.3 to 42.7; the warning regions are 25.3 to 28.2 and 39.8 to 42.7
69(31.9 %) Failed to respond .

7(3.2 %) Outliers -'
3( 1.4 %) Out of control •'
     but not an outlier


         Statistic
                               124(57.4 %) Within all limits
               Respondents
                                13(6.O %) In warning zone
                                        but within control
          Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
                    31.36
                     4.25
                    18.08
                    13.56
                    -7.76
                    -0.62
                    31.67
                    -6.86
                    -0.55
Grand Avg 31.45
             2.72
             7.41
             8.66
            -7.51
            -0.94
            31.67
            -6.86
            -0.86
11 (7.5 %) More than 3 norm. S.D. •.
12(8.2 %) Between 2 and 3 norm. S.D.'
                           .74(50.3 %) Within 1 norm. S.D.
                           •               of known value

                    5O(34.O %) Between 1 and 2 norm. S.D.

-------
36 /
50
\
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
Cesium-134
Lab
A
AA
AE
AF
AI
AJ
AK
AL
AO
AP
AIR
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
CS
CX
D
•'••••'W\'W£
[-.'•:'• P.,* •»
DD
DE
DG
DI
DL
DM
• =
03
Res. 1
34.0
30.0
32.0
33.0
31.0
34.0
32.0
37.0
32.0
34.0
27.0
37.0
31.0
32.0
51,0
31.0
34.0
33.0
33.0
32.0
31.0

17.0
30.0
32.0
32.0
--'•'<
32.0
37.0
15.0
31.0
32.0
30.0
32.0
33.0
33.0
30.0
32.0
28.0

27.0
33.0
Res. 2
35.0 .
31.0
33.0
32.0
31.0
35.0
33.0
44.0
34.0
33.0
30.0
36.0
33.0
30.0
54.0
30.0
33.0
34.0
31.0
31.0
32.0

>17.Q
30.0
33.0
34.0

35.0
33.0
16,0
34.0
32.0
26.0
32.0
33.0
30.0
30.0
32.0
26.0

30.0
33.0
Res. 3
34.0
33.0
33.0
31.0
31.0
34.0
32.0
41.0
31.0
31.0
27.0
34.0
32.0
30.0
X 47.0
31.0
33.0
32.0
32.0
31.0
34.0

v 18.0
32.0
32.0
31.0
' •••: f ,/ -.\, •
35.0
35.0
19.0
34.0
33.0
27.0
34.0
33.0
30.0
31.0
• 32.0
26.0
-
27.0
34.0
No data submitted
Insufficient
data
x =
Exper.
Sigma
0.58
1.53
0.58
1.00
0.00
0.58
0.58
3.51
1.53
1.53
1.73
1.53
1.00
1.15
3,51
0.58
0.58
1.00
1.00
0.58
1.53
X
0.58
1.15
0.58
1.53

1.73
2.00
2.08
1.73
0.58
2.08
1.15
0.00
1.73
0.58
0.00
1.15
•• "^ ;
1.73
0.58
Rng anal
(R + SR) Average
0.118
0.354
0.118
0.236
0.000
0.118
0.118
0.827
0.354
0.354
0.354
0.354
0.236
0.236
0.827
0.118
0.118
0.236
0.236
0.118
0.354

, 0.118
0.236
0.118
0.354
-
0.354
0.473
0.473
0.354
0.118
0.473
0.236
0.000
0.354
0.118
0.000
0.236
*
0.354
0.118
34.33
31.33
32.67
32.00
31.00
34.33
32.33
40.67
32.33
32.67
28.00
35.67
32.00
30.67
50.67
30.67
33.33
33.00
32.00
31.33
32.33

17.33
30.67
32.33
32.33
;' ^
34.00
35.00
16.67
33.00
32.33
27.67
32.67
33.00
31.00
30.33
32.00
26.67

28.00
33.33
TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known) Tag
1.00
-0.04
0.42
0.19
-0.15
1.00
0.31
3.19
0.31
0.42
-1.19
1.46
0.19
-0.27
.-; " 6;6S < - -
-0.27
0.65
0.54
0.19
-0.04
0.31

4.89
-0.27
0.31
0.31
''•'<.,. / '," :
0.88
1.23
',', -5.12 P;;:"
0.54
0.31
-1,31
0.42
0.54
-0.15
-0.39
0.19
-1.66

-1.19
0.65
IT s Above
!)• s Below
0.12
-0.92
-0.46
-0.69
-1.04
0.12
-0.58
2.31
t •
-0.58
-0.46
-2.08
0.58
-0.69
-1.15
5,77 °" * x'- ;:
-1.15
-0.23
-0.35
-0.69
-0.92
-0.58
•
-5.77 '• « x . '
-1.15
-0.58
-0.58
,'; ,'';>
-0.35
-0.58
-2.19
-0.46
-0.35
-1.04
-1.27
-0.69
-2.54
,•
-2.08
-0.23
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19-Apr
Cesium- 134
Lab
DO
DS
DT
DZ
E
EB
EH
EL

EO
EB
EV

EX
FE

FF-
FJ
FL
FN
FU
FZ
GE
GI
GQ
GT
GZ

HH
m
HK
HL
HP
HU
ex
I
IA
1C
ID
IE
It!
J
JE
JG
JH
JN
JQ
JS
JY
Res. 1
28.0
.
29.0
25.0
32.0
30.0
37.0
33.0

•v. s -
- " 1 , ^v
^ "• % --Xo t ,
^
^ ^ \
31.0


33.0
34.0
:. . ,
30.0
32.0
27.0
30.0
33.0




40.0
33.0
32.0
36.0
26.0
. ,,;;..
32.0
29.0
38.0



32.0
30.0
30.0



32.0
33.0
Res. 2 Res. 3
31.0
- -A" i "~ -
30.0
25.0
32.0
29.0
32.0
34.0

\--\->\ ' ->\ „ ,, '";•.'
^V?v>v\%;*
•;ft%;-; -"- v,^-'
v •• ^ * ^ V*1 s ^ .S
,-ix>, '" -v ;, /vr.
30.0

v" " r ~
30.0
33.0
s * -. \
29.0
32.0
30.0
29.0
33.0



X
47.0 v
31.0
31.0
38.0
26.0
s ^ ' ^ "•- •.-.'"'
31.0
27.0
36.0



31.0
31.0
30.0


V. 	 - •:::::•• ' . ,• . . T. •
32.0
30.0
28.0

34.0
27.0
31.0
30.0
40.0
32.0

^ ••"* s *
11 v* •.'"'U-'-'-.1';
\ \x s
s\-S X

30.0

% "
34.0
33.0

29.0
32.0
27.0
28.0
33.0




47.0
31.0
33.0
37.0
26.0
": - -: ^
34.0
27.0
35.0



32.0
31.0
23.0



33.0
32.0
• = No data submitted
0 s
Insufficient
data
x =
Exper.
Sigma
1.73

2.65
1.15
0.58
0.58
4.04
1.00

V ^
^ :\- , '~\>
v '"-^ "" ,1"
\*^ S

0.58


2.08
0.58
v< ; .
0.58
0.00
1.73
1.00
0.00

< •


4.04
1.15
1.00
1.00
0.00
1 "
1.53
1.15
1.53



0.58
0.58
4.04



0.58
1.53
•1994
37/50
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
0.354

0.591
0.236
0.118
0.118
0.945
0.236


x"1 '^ *- "••
v\ -,


0.118


0.473
0.118

0.118
0.000
0.354
0.236
0.000




0.827
0.236
0.236
0.236
0.000

0.354
0.236
0.354



0.118
0.118
0.827



0.118
0.354
29.00

31.00
25.67
31.67
29.67
36.33
33.00


;^ v;^ "*:s-^*;.
1 "'"- ^ * :'*,"'"^'-;l
"'••'' % "*
' - ,Xv?>--;:>,f
"'A ;*"vcvV%
^ '* °^ SV \ ' *'
-- •^,:''''VI
-0.39

'? >" -\TV-:^-\
0.31
0.65
'•. "^'•''^ '
-0.73
0.19
-1.19
-0.85
0.54
\ v ^
s
N \ \ S v*
s*"-
4.58
0.08
0.19
1.92
-1.89
" ' V- ''! -'
0.31
-1.31
1.69



0.08
-0.27
-1.31


^
0.31
0.08
ft = Above
& = Below
-1.73
- - *
-1.04
-2.89
-0.81
-1.50
0.81
-0.35

•'•;.'- • -
,.- '" C" ^-* '
\ s

; \ r •- >>' ,•'
-1.27

'. '••
-0.58
-0.23
V' «.. • .:,
-1.62
-0.69
-2.08
-1.73
-0.35
x " •
- *

•
3.70 x
-0.81
-0.69
1.04
-2.77
,-r - •
-0.58
-2.19
0.81
•
•
',• • •
-0.81
-1.15
-2.19
*
•/' • ;•:•••:*. :'
.--:..•:.•• ;;i',.' «.•••-
-0.58
-0.81
control limit
control limit

-------
38 /
50
Cesium-134
Lab Res. 1
K
KE
KM
KIT
KX
L
LF
, ' -
W ., ^ ^
3.06
0.00
0.58
0.00

'•> ' l
1.15
1.53
, ! ' ' •
1.00
.-, -i '
0.58 .

---*-, :,
0.58

0.00
2.08
2.00

0.58
\ __ -.
;s "" *fj '
"->i ,\ ' ';
0.58

0.00
1.53
0.58
0.58
1.53
0.58

Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
0.236

0.118
• •{•'
0.236
0.118
0.354


0.709
0.000
0.118
0.000


0.236
0.354

0.236
* ^
0.118

',, ^
0.118
,,
0.000
0.473
0.473

0.118


', '•;
0.118

0.000
0.354
0.118
0.118
0.354
0.118

29.00
,
30.33
'-. - ''• •-,- * 'V
, 31.00
34.33
32.00
;-"- _ , ."'- -_ "^

45;33 ;
31.00
28.67
35.00

< " "" ''•
33.33
28.33
*
33.00
- "" \ "• v t
31.33
* ; ' *i • , > '
~ "", - v N' -1 ,*•"
30.67

29.00
34.33
24.00

35.67


;' "' ":'
36.33

30.00
37.67
~ 29.67
26.67
33.33
30.67

TAG SYMBOLS
Determined
to be an
outlier
-0.85
• ' , - ^ ', , x- '
-0.39
' v//- "'-"-"V1
-0.15
1.00
0.19
\V;.v^O '.,;
'> , ''"'', ;
4.8;t \
-0.15
-0.96
1.23

"• V S1" *
0.65
-1.08

0.54

-0.04

^ ^ t
-0.27
'.„ , ">:* '"-'\ '
-0.85
1.00
-2.58

1.^16

SJ ' ' ''
' ". " '••" *," *
1.69

-0.50
2.16
-0.62
-1.66
0.65
-0.27

IT =s Above
U =i Below
-1.73
";,, '/. •'• - '
-1.27
-; -: • -'.• ,
-1.04
0.12
-0.69
"' ?,*.*•. ' *
' " / ,*'•"'
3;03 ;;,': x
-l!o4
-1.85
0.35
'* ; ' *
'_-'''•' *
-0.23
-1.96
* *"
-0.35
- , , *
-0.92
' 
-------
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
39
/50
Cesium- 134
Lab
Pf
PV
PW
PY
Q
QC
QJ
QK
QL
QP
QQ
QT
QU
QW
QX
QY
QZ
RC
RD
RE
RF
RG
RJ
RK
RL
RM
RP
RR
RV
RZ
S
sc
SD
SF
SI
SL
SM
SO
SR
ss
ST
SW
sx
sz
T
Res. 1
13.0
31.0
30.0
28.0

28.0
34.0
30.0
31.0

32.0
18.0
23.0
32.0
*
30.0
24.0


35.0



29.0

31.0
25.0
33.0
33.0
28.0
35.0
30.0
32.0

29.0

32.0
32.0
30.0
32.0
38.0
31.0
33.0
Res. 2
15.0
32.0
30.0
28.0
11 ._" ,_ ^v"-?..
31.0
35.0
26.0
24.0
< ^x
31.0
21.0
30.0
31.0
\
29.0
26.0
s
<• 'x
33.0

^
<
35.0

31.0
25.0
33.0
33.0
31.0
35.0
28.0
33.0

29.0

30.0
29.0
30.0
32.0
39.0
30.0
32.0
Res. 3
, 13.0
30.0
30.0
\ -" - , s* -
30.0

27.0
36.0
27.0
34.0
^
31.0
20.6'
18.0
32.0
27.0
25.0
s

30.0

<

33.0
.
33.0
26.0
33.0
33.0
27.0
34.0
30.0
33.0

29.0

31.0
30.0
30.0
31.0
35.0
31.0
32.0
• s No data submitted
0 =
Insufficient
data
x s
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known)
1.15
1.00
0.00
1.15

2.08
1.00
2.08
5.13

0.58
1.53
6.03
0.58
1.53
1.00
-

2.52

•-

3.06

1.15
0.58
0.00
0.00
2.08
0.58
1.15
0.58

0.00

1.00
1.53
0.00
0.58
2.08
0.58
0.58
0.236
0.236
0.000
0.236
.-V '
0.473
0.236
0.473
1.345
s
0.118
0.354
1.795
0.118
0.354
0.236


0.591

v

0.709

0.236
0.118
0.000
0.000
0.473
0.118
0.236
0.118

0.000

0.236
0.354
0.000
0.118
0.473
0.118
0.118
13.67
31.00
30.00
28.67
•- ••** - ' "' "-
28.67
35.00
27.67
29.67
N '
31.33
19.67
23.67
31.67
28.67
25.00
^
* \
32.67



32.33
s
31.67
25.33
33.00
33.00
28.67
34.67
29.33
32.67

29.00

31.00
30.33
30.00
31.67
37.33
30.67
32.33
TAG SYMBOLS
Determined
to be an
outlier
•6,16- x
-0.15
-0.50
! " •• J \*
:0.96

-0.96
1.23
-1.31
-0.62
<
-0.04
-4.08
-2.69
0.08
-0.96
-2.23
"
*•
0.42
•s-
v \
•*
0.31

0.08
-2.12
0.54
0.54
-0.96
1.12
-0.73
0.42
' • '""-?••.'
-0.85

-0.15
-0.39
-0.50
0.08
2.04
-0.27
0.31
IT = Above
Ji = Below
-7.04
-1.04
-1.39
,!i
-1.85
- - ' , >:
-1.85
0.35
-2.19
-1.50

-0.92
-4.97
-3.58
-0.81
-1.85
-3.12
s v A

-0.46

-

-0.58

-0.81
-3.00
-0.35
-0.35
-1.85
0.23
-1.62
-0.46

-1.73

-1.04
-1.27
-1.39
-0.81
1.15
-1.15
-0.58
control
control
Tag
X

9

= • • -




•

X
Ji
«

U
• '
•

•
*
•

' •








« •

; ••".







limit
limit

-------
40/50
EMSL-LV Performance Evaluation: Blind-B,
19-Apr-1994
•
Cesium-134

Lab
TA
TD
TE

TG
TH
n
TL
••TN / '

TQ
TS
TU
TY
U
UA
UE
UG
UK
UN
UP
UQ
uw
UY
VA
VC
VG
vr
VOf

VM

VN
vo
VQ
VT
W
WA
X
Z

Res. 1
31.0
33.0
29.0


34.0
32.0
36.0


32.0
29.0
32.0

34.0
v ' ' f
\
34.0

29.0
34.0
26.0
„, " ,- /•
36.0
32.0


30.0
1 v " -




t
29.0

31.0
29.0
30.0
30.0
32.0

Res. 2
31.0
28.0
30.0


33.0
31.0
30.0


32.0
28.0
30.0

35.0

33.0

41.0
34.0
30.0

36.0
31.0


31.0
,





34.0

34.0
34.0
31.0
30.0
31.0


Res. 3
31.0
31.0
30.0




33.0
32.0
29.0




30.0
30:0
32.0


34.0


34.0


35.0
33.0
33.0


36.0
29.0




32.0












30.0
• ", '

38.0
32.0
30.0
31.0
31.0
Data
Average
13.67
16.67
17.33
19.67
23.67
24.00







Tag
X
X
X
X
li
li
Lab
PT
CM
BW
QU
QW
NO
Exper.
Sigma
0.00
2.52
0.58

- \ ,
0.58
0.58
3.79

?
1.15
1.00
1.15

0^58

0.58

6.00
0.58
3.51
/ ;
0.00
1.53
j. ''

1.00






2.65

3.51
2.52
0.58
0.58
0.58
Rng anal
(R + SR)
0.000
0.591
0.118


0.118
0.118
0.827


0.236
0.236
0.236

0.118
-'• , ' /
0.118

1.795
0.118
0.827
^
0.000
0.354


0.236
*



1 _,

0.591

0.827
0.591
0.118
0.118
0.118
' Normalized deviation
Average
31.00
30.67
29.67
; , *



33.33
31.67
31.67




31.33
29.00
31.33


34.33


33.67

I
35.00
33.67
29.67


36.00
30.67




31.00




; •• s




^


31.00


34.33
31.67
30.33
30.33
31.33
(grand-avg) (known) Tag
-0.15
-0.27
-0.62


0.65
0.08
0.08
> '••

-0.04
-0.85
-0.04
_- : •; : -^ • ;
1.00
V \ - •* S , • - ' ,-
0.77

1.23
0.77
-0.62
1 -, V * ' •
1.58
-0.27

- - '>." - "' j •
-0.15
; , - ' - , ,- -
' -.- '" ' ', X ',''




-0.15
.': -"- ": /s ,-,":
1.00
0.08
-0.39
-0.39
-0.04
-1.04
-1.15
-1.50

'' -\ ' " •" '
-0.23
-0.81
-0.81
• .- •'•'-'•

-0.92
-1.73
-0.92
.C7 •<'•• ; ••• \
0.12 ,
•\t.,\*\< • :
-0.12
' "" , '-,' - •
0.35
-0.12
-1.50
*'::' •••','•
0.69
-1.15
( \,f ••* "" „. ' f * •""••
••v '"/ '•--'• •••:
-1.04
, „' ~ »
j f ' J '' *
,. \ ' ;,.»....
; ' *'
- - •<
"• •• ' ^
' :. '- *:;
-1.04
-\\ ?- V* '
0.12
-0.81
-1.27
-1.27
-0.92
sorted by Laboratory Average
Average






• = No data submitted
0 = Insufficient data
X
25.00
25.33
25:67
26.00
26.67
26.67
Tag
U





Lab
RC
RV
DZ
HU
PM
DG
Average Tag Lab






TAG SYMBOLS
= Determined to be an outlier
27.67
27.67
27.67
27.67
28.00
28.00
1T =5 Above
li = Below
QL
JG
IA
CQ
GE
DL
control limit
control limit

-------


Cesium-134

Average
28.00
28.33
28.67
28.67
28.67
28.67
28.67
29.00
29.00
29.00
29.00
29.00
29.00
29.33
29.33
29.67
29.67
29.67
29.67
29.67
30.00
30.00
30.00
30.33
30.33
30.33
30.33
30.33
30.33
30.67
30.67
30.67
30.67
30.67
30.67
30.67
30.67
30.67
31.00
31.00
31.00
31.00
31.00
• = No data

EMSL-LV Performance

Data sorted
Tag Lab
AW
MQ
SC
QZ
QJ
Q
M
TS
SM
NJ
K
GI
DO
SF
FU
UP
TE
QP
PI
EB
ST
PW
PB
X
WA
ss
KM
FE
DD
UY
TD
SZ
PQ
NH
JE
C
BH
BC
VO
VG
TA
SR
PV
Average
31.00
31.00
31.00
31.00
31.00
31.33
31.33
31.33
31.33
31.33
31.33
31.33
31.67
31.67
31.67
31.67
31.67
31.67
31.67
31.67
31.67
31.67
32.00
32.00
32.00
32.00
32.00
32.00
32.00
32.33
32.33
32.33
32.33
32.33
32.33
32.33
32.33
32.33
32.33
32.33
32.67
32.67
32.67

Evaluation: Blind-B, 19-Apr-1994

by Laboratory Average
Tag Lab
LT
KX
DT
D
AI
Z
TU
TQ
QT
N
BN
AA
W
TL
TI
SW
RR
QX
JY
J
HK
E
LF
HL
FZ
DE
BM
BA
AF
T
RM
JS
I
FJ
CP
CE
CA
BO
AP
AK
SI
RF
CS
Average
32.67
32.67
33.00
33.00
33.00
33.00
33.00
33.00
33.00
33.00
33.33
33.33
33.33
33.33
33.33
33.33
33.67
33.67
34.00
34.33
34.33
34.33
34.33
34.33
34.33
34.67
35.00
35.00
35.00
35.00
35.67
35.67
36.00
36.33
36.33
36.33
37.00
37.33
37.67
40.67
44.67
45.33
50.67
submitted TAG SYMBOLS fl =
0 = Insufficient data x = Determined to be an outlier li =

41/50


Tag Lab
AU
AE
S
RZ
MV
GQ
EL
CX
CO
BL
TH
PP
MP
FL
DM
BK
UN
UE
CJ
VT
U
NK
L
AJ
A
SD
UK
QK
MA
CK
O
AZ
UW
P
1C
EH
HP
sx
PC
AL
x ffl
x LR
x BG
Above control limit
Below control limit

-------
42/50          EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994

Cesium-134

 % responding labs    	   Frequency distribution

 10-
.Tli.lllllf I...
     -6     '      -4           -2           6           +2     "      +4           +6
                    Normalized deviation of the mean from the known value
 % responding labs   	Frequency distribution
 10-
                          .  -T .••!•hlflilj•.
     -6           -4            -2           0           +2,           +4           +6
                   NormaUzed deviation of the mean from the grand average

-------
                  EMSL-LV Performance Evaluation: Blind-B,  19-Apr-1994
                                   43/50
Cesium-137                          Statistical Summary                       216 Participants
The known value of this nuclide is 29.0 pCi/1 with an expected precision of 5.0; the control limits
are 20.3 to 37.7; the warning regions are 20.3 to 23.2 and 34.8 to 37.7
69(31.9 %) Failed to respond .
8(3.7 %) Outliers **
1(O.5 %) Out of control
     but not an outlier

         Statistic
                132(61.1 %) Within all limits

Respondents
6(2.8 %) In warning zone
        but within control

          Non-outliers
Mean
Std. Dev.
Variance
% Coef. of Var.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value

Norm. dev. of median from known value
30.98
4.29
18.41
13.85
6.82
0.46
31.00
6.90

0.47
Grand Avg 31.17
2.40
5.76
7.70
7.48
0.90
31.00
6.90

0.83
9(6.1 %) More than 3 norm. S.D.
             84(57.1 %) Within 1 norm. S.D.
                            of known value
6(4.1 %) Between 2 and 3 norm. S.D. •
     48(32.7 %) Between 1 and 2 norm. S.D.

-------
44/50
Cesium-137
Lab Res. 1
A
AA
AE
AF
AI
AJ
AK
AL
AO
AP
AR
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CO
CJ
CK
CM
CO
CP
CQ
CS
CX
D
DB
DD
DE
DG
DI
DL
DM
• =
0 =
31.0
31.0
31.0
33.0
29.0
35.0
33.0
35.0
1 •
32.0
' ' \'',- - '-\
34.0
31.0
33.0
27.0
32.0
29.0
32.0
32.0
31.0
32.0
31.0
35.0
17.0
30.0
31.0
32.0
32.0
35.0
26.0
29.0 ,
24.0
29.0
32.0
33.0
32.0

31.0
32.0
32^0

28.0
33.0
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
Res. 2
31.0
32.0
32.0
29.0
31.0
34.0
33.0
31.0

28.0
1 \ <;. / >•
33.0
35.0
32.0
30.0
32.0
39.0
31.0
31.0
30.0
32.0
31.0
34.0
17.0
30.0
32.0
31.0
33.0
33.0
26.0
31.0
24.0
31.0
33.0
31.0
30.0

31.0
33.0
29.0

33.0
33.0
Res. 3
31.0
29.0
33.0
34.0
31.0
35.0
35.0
29.0

30.0
- ~ '
33.0
32.0
35.0-
32.0
31.0
28.0
29.0
33.0
30.0
32.0
31.0
32.0
26.0
29.0
31.0
30.0
37.0
33.0
31.0
35.0
25.0
33.0
34.0
34.0
29.0

31.0
33.0
29.0
. *
29.0
31.0
No data submitted
Insufficient
data
x =

Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
0.00
1.53
1.00
2.65
1.15
0.58
1.15
3.06
' ' - ' •/' -
2.00
,;-••-
0.58
2.08
1.53
2.52
0.58
6.08
1.53
1.00
0.58
0.00
. 0.00
1.53
5.20
0.58
0.58
1.00
N
2.65
1.15
2.89
3.06
0.58
2.00
1.00
1.53
1.53 .

0.00
0.58
1.73

2.65
1.15
0.000
0.354
0.236
0.591
0.236
0.118
0.236
0.709
i
0.473

0.118
0.473
0.354
0.591
0.118
1.570
0.354
0.236
0.118
0.000
0.000
0.354
1.120
0.118
0.118
0.236
0.591
0.236
0.591
0.709
0.118
0.473
0.236
0.354
0.354

0.000
0.118
0.354

0.591
0.236
31.00
30.67
32.00
32.00
30.33
34.67
33.67
31.67
* * i "
30.00
^'•c /-'•'• ',
33.33
32.67
33.33
29.67
31.67
32.00
30.67
32.00
30.33
32.00
31.00
33.67
20.00
29.67
31.33
31.00
34.00
33.67
27.67
31.67
24.33
31.00
33.00
32.67
30.33

31.00
32.67
30.00
'""
30.00
32.33
TAG SYMBOLS
Determined to
be an
outlier
-0.06
-0.17
0.29
0.29
-0.29
1.21
0.86
0.17

-0.41
' <• " ' '
0.75
0.52
0.75
-0.52
0.17
0.29
-0.17
0.29
-0.29
0.29
-0.06
0.86
-3.87
-0.52
0.06
-0.06
0.98
0.86
-1.21
0.17
-2.37
-0.06
0.63
0.52
-0.29

-0.06
0.52
-0.41

-0.41
0.40
ft = Above
•U s Below
0.69
0.58
1.04
1.04
0.46
1.96
1.62
0.92
, s 7- , •;,,
0.35
,\ . «/ - \*
1.50
1.27
1.50
0.23
0.92
1.04
0.58
1.04
0.46
1.04
0.69
1.62
\ ' l *
,t3il2 x
0.23
0.81
0.69 ,
1.73
1.62
-0.46
0.92.
-1.62
0.69
1.39
1.27
0.46
- " *
0.69
1.27
0.35
: - S ' • '
0.35
1.15
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
45/50
Cesium-137

Lab
DO
'•DS">:;
DT
DZ
E
EB
EH
EL
'"EOf,
EB :
^:EXr
FE
FJ
FL
FK
FU
FZ
GE
GI
GQ
GT

GZ
HI
HK
HL
HP
HU
HX
I
IA
1C
ID
IE
IU
J
JE
JG
JH
JN
JQ
JS
JY
• =
0 s

Res. 1
34.0
""s "" •• \ ' "• ~" -.XX '''•''
37.0
26.0
32.0
31.0
28.0
30.0
",^ H- ^7 :'
'..- -.^ft-s
' ;''lHv\xC<:
28.0
33.0
32.0

30.0
33.0
28.0
31.0
32.0
>. _

-
47:0
32.0
32.0
35.0
24.0
X « ^ -v-\ .,\Y
32.0
33.0
31.0



31.0
31.0
28.0



30.0
33.0

Res. 2
27.0
•-xiv'"!VTj> vY
33.0
28.0
32.0
31.0
29.0
29.0
\:;^s!v '-
^;%Sl;J
!i^^:=
29.0
30.0
32.0
s
30.0
32.0
33.0
31.0
32.0
v

X ^ *
45.0
33.0
32.0
39.0
24.0
r;vC>;^tV
29.0
31.0
34.0



31.0
30.0
26.0



32.0
34.0

Res. 3
28.0
"r;"Ml:^;;"
30.0
26.0
30.0
31.0
30.0
28.0'
^:;K~''^C--
|g^k:>^r:
V v"->f'-iV ' ';'" -'
26.0
33.0
33.0

29.0
33.0
29.0
30.0
32.0


v ^
49.0
32.0
33.0
37.0
24.0
^v;--"-1 ;;"%' •• ^<"
32.0
31.0
31.0



31.0
31.0
28.0



32.0
33.0
No data submitted
Insufficient
data
x =
Exper.
Sigma
3.79
" * ^" % -
3.51
1.15
1.15
0.00
1.00
1.00

"" •• • •• ""
"• "" ^ ^ " s S\ " ^
^ ^ 1 S
:iv?:r ;-/
' JL53^
1.73
0.58

0.58
0.58
2.65
0.58
0.00



2.00
0.58
0.58
2.00
0.00
>-•'•- :>, ~ '„
1.73
1.15
1.73



0.00
0.58
1.15



1.15
0.58
Rnganal
(R + SR)
0.827
^\rX/':%-!\
0.827
0.236
0.236
0.000
0.236
0.236
" > r^vV^ '
- '\Si}£r:
^\ U ; ;.;,';';,-;,
0.354
0.354
0.118
<
0.118
0.118
0.591
0.118
0.000


- '* >
0.473
0.118
0.118
0.473
0.000
; -x -'^
0.354
0.236
0.354



0.000
0.118
0.236


' • •• ' ' '.' v ""'..'..:''• - • '
0.236
0.118
Normalized deviation
Average
29.67
V-" ^ ^ Nl- f^""''
33.33
26.67
31.33
31.00
29.00
29.00
- > I;L^'>:-
Jv3^|
s, "; t''^, >-•"--/
7^27leV'
32.00
32.33
\
29.67
32.67
30.00
30.67
32.00


-ll -' ;V-;^ ,.
47.00
32.33
32.33
37.00
24.00
%;iV -:^:J
31.00
31.67
32.00
*


31.00
30.67
27.33


s
31.33
33.33
TAG SYMBOLS
Determined
to be an outlier
(grand-avg) (known) Tag
-0.52
VX; -.•• ^' ;"•"; v ^5Xv-,^\f;J^s\'.
vx^ •• ^ ^ ^x ^ ^" ^^ ^ ? s '•• ^
0.75
-1.56
0.06
-0.06
-0.75
-0.75
,,0'AS'>^Xv;.';>
>ff^||^;.
^c^CS^^
jljl^^ _
0.29
0.40
* s
-0.52
0.52
-0.41
-0.17
__0.29 _
t"-\\--:v^-?y-:\ .

*;"-»> ; '^^r -
FM6;4^r
0.40
0.40
2.02
	 j2.48 	
^;\5v:;Wvf;V::
-0.06
0.17
0.29
^


-0.06
-0.17
-1.33



0.06
0.75
1T s Above
& = Below
0.23
V^&V:?V?'
1.50
-0.81
0.81
0.69
0.00
0.00
j />;••;•• ,; *;
U&\r~":V> ,' '"*"' ,.
-0.46
1.04
1.15
«,
0.23
1.27
0.35
0.58
1.04
' "*: *

'" vT'. *
- e.24 • xo«.
1.15
1.15
2.77
-1.73
;C^s7x"7'>-;
0.69
0.92
1.04
*
•
•
0.69
0.58
-0.58
•
«
.- «.
0.81
1.50
control limit
control limit

-------
46/50
11
EMSL-LV Performance Evaluation: Blind-B, 19- Apr- 1994
Cesium-137

Lab
K
-KE*
KM
KT
KX
L
LF
LG
LL
LM
LR
LT
M
MA
;MN

MO
MP
MQ

MS
MV
MY
N
NA
NG*
NH
NI
NJ
NK
NO
NT
O
OF
OS
OX
OY
P
PA
PB
PC
PG
PI
PM
PP
PQ
PR

Res. 1
35.0
'• "~>
29.0
f
29.0
31.0
31.0
•• j <

, -" ', > "
28.0
32.0
29.0
35.0
i.

s ' %
25.0
29.0


32.0

31.0

-
33.0

. 49,0
31.0
15*0
, -
34.0
;



41.0

31.0
35.0

31.0
32.0
28.0
32.0
" "

Res. 2
38.0
/- -- •'•' -
28.0

31.0
30.0
30.0

"""•,,,.
•. .... \ -. .... •• •. -. ^
32.0
32.0
30.0
35.0


,"' * *" *••• '•'''••••,'•'
30.0
32.0


32.0
-, -
31.0


33.0
* :
51.0
31.0
14.0

34.0
• v^ :'
/ ":
'; , .." '
'• , >
43,0

32.0
37.0

29.0
29.0
31.0
32.0
•" '-, *''"' '•'

Res. 3
37.0
:~l'r>'': 'c' ' -
30.0

31.0
29.0
29.0

•• - * ' v, * ••'
,v~.v. \ V...N\ :-.: :f f:: -.-.^
30.0
32.0
30.0
33.0


\- - ^^ ' ?
27.0
30.0


33.0

32.0
-' '-,' ~i'>

33.0

51.0
29.0
15.0

34.0
~ "• ."

-* :' ''-, ' ' •

44.0

29.0
39.0
\
30.0
28.0
30.0
34.0
' s - " f , "
• s= No data submitted
0 =
Insufficient
data
x =
Exper.
Sigma
1.53
* ' ,.' -
1.00

1.15
1.00
1.00
!< ,-_
, " ^ , ,
" r \ t
2.00
0.00
0.58
1.15


-•.;•• ' ,," , ;
2.52
1.53
.. *

0.58

0.58
- " ' .'

0.00

"> , 1^15^-
1.15
0,58
,"•'''- ' :
0.00
O1-


> ' -
1.53

1.53
2.00

1.00
2.08
1.53
1.15

Rng anal
(R + SR)
0.354

0.236

0.236
0.236
0.236



0.473
0.000
0.118
0.236



0.591
0.354

J ^
0.118

0.118

<<• ,
0.000

0.236 :
0.236
0.118

0.000


,
' ',
0.354

0.354
0.473

0.236
0.473
0.354
0.236

Normalized deviation
Average
. 36.67
, - *~
29.00

30.33
30.00
30.00



30.00
32.00
29.67
34.33



27.33
30.33


32.33

31.33

.*' „ ' ''"
33.00
.
50.33
30.33
14,67

34.00

; • -


42.67

30.67
37.00

30.00
29.67
29.67
32.67
'
TAG SYMBOLS
Determined
to be an outlier
(grand-avg) (known) Tag
1.90
' '•. ' ' ' *, 'V """ ^
-0.75
•. •»
-0.29
-0.41
-0.41

'"' *** ?' • ;>
, - • , ','••• ^-i- "
-0.41
0.29
-0.52
1.10


* •.'•
-1.33
-0.29


0.40

0.06
j ^ 5 •• -.
^ "" •, ••
0.63

6.64
-0.29
' ' -SM % ' '

0.98

' : -'
~t ^., - f •«•

3.98

-0.17
2.02

-0.41
-0.52
-0.52
0.52
** / , , '*
1T = Above
•li = Below
2.66
\-., ', V '»
0.00
' ' ' 1 •
0.46
0.35
0.35
s >. ^ ^ %
- > - , ;'' > • -
-:*' *-\ - » -
0.35
1.04
0.23
1.85
' • '-
'",""' '•'•<,-

-0.58
0.46

•\ . -I- -•---,
1.15
'•'-"-" { '•'
0.81
•:•:•'. .*.*.y
'/'.; ,"'- v «V;-
1.39
; , ' - ,^ »'
;7.39;^"x/.
0.46
*4.97 X
\"' ^;-,- - * „
1.73
^''..p' «;; '
'' '- • ' '*,;*
'• :'~j /',->;';
: -'•-'•
4.73 , x
, •
0.58
2.77
- •• •
0.35
0.23
0.23
1.27
- > - - , * -•'
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 19-Apr-1994
Cesium-137
Lab Res. 1
PT
PV
PW
PY
Q
QC
QJ
QK
QL
QP
QQ
QT
QU
QW
QX
QY
QZ
RC
RD
RE
RF.x

RG
RJ

RK
RL
RM
RP
RR
RV
RZ
S
sc
SD
SF
SI
SL
SM
SO
SR
ss
ST
SW
sx
sz
T
• v-;"i4o--
32.0
31.0
'K >*s; ''"V"-
29.0
.. ^ ^ ..V... .. ^ ., .. S^A
28.0
30.0
32.0
27.0
f - - ^ ---* V\
30.0
16.6 S
29.0
33.0
'- ' .", " '
30.0
29.0
, ,• v >^ ^ „ -
•^-'' '" , , !%" ''
13.0

*' "•
,' "''-'• ' V"



28.0

31.0
29.0
30.0
27.0
30.0
34.0
32.0
33.0

29.0

31.0
33.0
30.0
33.0
35.0
31.0
30.0
Res. 2
16,0
28.0
32.0
's '** -^ ' '' \ \ ^
29.0
J£"\'*V -V ;V
32.0
28.0
30.0
37.0
•- vs " ^ •- ^ %V "•• %
29.0
v' -2110- '< '
25.0
35.0
,V __ sv -x " * -
30.0
32.0
'•'''*"'" ^ ^ s i
" ' o-'s
~-'- '\14.0' ' '

^' \! "-\ x- ; •
,'/ < * * ^^ ^ ^ '

^\ v%-; -\v
'; •• " ' ^
27.0

31.0
30.0
31.0
29.0
31.0
40.0
28.0
33.0

29.0

29.0
30.0
29.0
33.0
35.0
30.0
30.0
Res. 3
>:14.0 <
31.0
31.0
\-.^"-. " "
29.0
• \;-,,^l!i\:
35.0
29.0
32.0
32.0
>,-\ v *,;,,,
30.0
1*7,0
30.0
34.0
-
30.0
27.0

-v*" ,.,
14;0


\-. *

- ; J ' ^,\
"c"^'- -,
27.0

32.0
30.0
30.0
27.0
32.0
32.0
28.0
32.0

30.0

25.0
34.0
31.0
33.0
33.0
31.0
32.0
• s No data submitted
0 3
Insufficient, data x =
Exper.
Sigma
1.15
2.08
0.58
•- s \
0.00
'-" . / .; o\,~ '
3.51
1.00
1.15
5.00
X
0.58
c- '2,65 -
2.65
1.00

0.00
2.52


0»68

-



x ' ^
0.58

0.58
0.58
0.58
1.15
1.00
4.16
2.31
0.58

0.58

3.06
2.08
1.00
0.00
1.15
0.58
1.15
47/50
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
0.236
0.473
0.118
•• •• v -.
0.000
-' - ".'"
0.827
0.236
0.236
1.345
•\ ''^
0.118
0;S91
0.591
0.236

0.000
0.591


6.118






0.118
\
0.118
0.118
0.118
0.236
0.236
0.945
0.473
0.118

0.118

0.709
0.473
0.236
0.000
0.236
0.118
0.236
1467 ;
30.33
31.33
- ' '- '\' ,: f "«,
29.00
^-- , - ,,-.-• ''.\*;
31.67
29.00
31.33
32.00
i ' -' :,-~\^ -•'
29.67
-. V >>18.0&'vV
28.00
34.00

30.00
29.33
'-. \"-\ '. *-" '' '- * \s
C ' " * '" \r ^
''.'• -:.i^67/ -:

-^ ; ;\ '/--
'\' x' ^ " -\,^


v,-\- ;'-\" '^--: -
27.33
*
31.33
29.67
30.33
27.67
31.00
35.33
29.33
32.67

29.33

28.33
32.33
30.00
33.00
34.33
30.67
30.67
TAG SYMBOLS
Determined
to be an
outlier
--! l%!,-\ '"
-0.41
-0.64
^ >. s^ * •*• v % "^ + "
:l'. :-u^-V-
**Ov^& -• 5 '"""
^ C1 -* i •• \X "" •* ^ % f

^ /• ^ v
11 v \ v \ ••"
; - ;4f .. \,'
.,,-.-* -,-v' l>^'\
-1.33
:"v ' '" -
0.06
-0.52
-0.29
-1.21
-0.06
1.44
-0.64
0.52

-0.64

-0.98
0.40
-0.41
0.63
1.10
-0.17
-0.17
ft = Above
li = Below
,4*97-: :vx'
0.46
0.81
.. ^ ^ -%, ^ ^^
0.00
s \ -' s SX'-
v; " " ss% ^ ; • -„,
0.92
0.00
0.81
1.04
;;:"°' r <•>.<
0.23
%8l^ ;-'x ^
-0.35
1.73
;-;^:v--:^v >•
0.35
0.12
v'c :'v-^ '••*'-
-" •''"' '' 'V ", • '
>5,3l^'\ xf'

- " * V
;/ / '-- \«x^

! ;,-- V' / !* ,""•
>- •• : - , , '• ':
-0.58
;>, -- y'^
0.81
0.23
0.46
-0.46
0.69
2.19
0.12
1.27

0.12

-0.23
1.15
0.35
1.39
1.85
0.58
0.58
control limit
control limit

-------
f 48 / 50
I
Cesium
Lab
TA
TD
TE
TG
TH
TI
TL
TN -
TQ
TS
TU
TY
U
UA
UE
UG
UK
UN
UP
UQ
uw
UY
VA
vc
VG
VI
VJ
VM
VN ,
vo
VQ
VT
W
WA
X
Z
EMSL-LV Performance Evaluation: Blind-B,
•137
Res. 1
32.0
36.0
31.0

33.0
34.0
20.0

31.0
30.0
34.0

33.0

32.0

41.0
36.0
29.0

31.0
32.0

-
32.0




33.0

31.0
29.0
31.0
30.0
32.0

Res. 2
34.0
32.0
28.0

33.0
33.0
20.0

34.0
29.0
32.0
- *
33.0

33.0

40.0
34.0
32.0

32.0
28.0


28.0




31.0

34.0
26.0
31.0
31.0
32.0


Res. 3
30.0
33.0
31.0


34.0
33.0
25.0


28.0
29.0
34.0


34.0


34.0


40.0
36.0
34.0


30.0
29.0
s



30.0








30.0


37.0
27.0
31.0
31.0
30.0
Data
Average
13.67
14.67
14.67
18.00
20.00
21.67







Tag
X
X
X
X
X

Lab
RF
PT
NO
QU
BW
TL

Exper.
Sigma
2.00
2.08
1.73

0.58
0.58
2.89
f
3.00
0.58
1.15

0.58

1.00
/ -
0.58
1.15
2.52

1.00
2.08


2.00




1.53
",
3.00
1.53
0.00
0.58
1.15

Rng anal
(R + SR)
0.473
0.473
0.354

0.118
0.118
0.591

0.709
0.118
0.236

0,118

0.236

0.118
0^236
0.591

0.236
0.473


0.473




0.354

0.709
0.354
0.000
0.118
0.236

19-Apr-1994

Average
32.00
33.67
30.00


33.33
33.33
21.67


31.00
29.33
33.33


33.33


33.00


40.33
35.33
31.67


31.00
29.67




30.00








31.33


34.00
27.33
31.00
30.67
31.33

Normalized
(grand-avg)
0.29
0.86
-0.41

0.75
0.75
-3.29

-0.06
-0.64
0.75

0.75

0.63

3.17
1.44
0.17
- •'
-0.06
-0.52


-0.41




0.06

0.98
-1.33
-0.06
-0.17
0.06
"*
deviation
(known) Tag
1.04
1.62 -
0.35
• ' ''-•''
1.50
1.50
-2.54
. -
0.69
0.12
1.50
,• • ' ': .*
1.50
*
1.39
." -'--•*
3.93 ft
2.19
0.92
'»
0.69
0.23
' \ ' '•
, ' ' ;•',
0,35
\ , . • '
•
*
, •
0.81
' ' ' *
1.73
-0.58
0.69
0.58
0.81
sorted by Laboratory Average
Average






• s No data submitted
0 = Insufficient data
X
24.00
24.33
26.67
27.33
27.33
27.33
Tag






Lab
HU
CP
DZ
W
RM
MP
Average Tag Lab






TAG SYMBOLS
= Determined to be an outlier
27.33
27.67
27.67
27.67
28.00
28.33
JG
S
FE
CM
QW
SR
ft s Above control limit
•li = Below control limit

-------


EMSL-LV Performance
Cesium-137

Average Tag
29.00
29.00
29.00
29.00
29.00
29.33
29.33
29.33
29.33
29.67
29.67
29.67
29.67
29.67
29.67
29.67
29.67
29.67
29.67
30.00
30.00
30.00
30.00
30.00
30.00
30.00
30.00
30.00
30.00
30.00
30.00
30.33
30.33
30.33
30.33
30.33
30.33
30.33
30.33
30.67
30.67
30.67
30.67
• = No data submitted
. 0 = Insufficient data
v* 	

Data sorted
Lab
QK
Q
KM
EL
EH
TS
SM
SF
RC
UY
RV
QT
PP
PM
M
FU
DO
C
BA
VG
TE
ST
QZ
PI
LR
LF
L
GE
DL
DG
AP
RZ
PV
NK
MQ
KX
D
BL
AI
X
T
SZ
PB
Average
30.67
30.67
30.67
30.67
31.00
31.00
31.00
31.00
31.00
31.00
31.00
31.00
31.00
31.00
31.00
31.00
31.33
31.33
31.33
31.33
31.33
31.33
31.33
31.33
31.33
31.67
31.67
31.67
31.67
31.67
31.67
32.00
32.00
32.00
32.00
32.00
32.00
32.00
32.00
32.00
32.00
32.00
32.33

Evaluation: Blind-B, 19-Apr-1994

by Laboratory Average
Tag Lab
JE
GI
BH
AA
WA
UW
TQ
SC
J
I
EB
DD
CQ
CE
BN
A
Z
VO
RR
QL
PW
N
JS
E
CA
UP
QJ
IA
CO
BC
AL
TA
QP
LT
1C
GQ
FJ
BM
BK
BG
AF
AE
SS
Average
32.33
32.33
32.33
32.33
32.33
32.67
32.67
32.67
32.67
32.67
32.67
33.00
33.00
33.00
33.00
33.33
33.33
33.33
33.33
33.33
33.33
33.33
33.33
33.67
33.67
33.67
33.67
34.00
34.00
34.00
34.00
34.33
34.33
34.67
35.33
35.33
36.67
37.00
37.00
40.33
42.67
47.00
50.33
TAG SYMBOLS IT s
x s Determined to be an outlier li =

49/50


Tag Lab
MV
HL
HK
FL
DM
SI
PQ
FZ
DE
CX
AW
UE
SW
NH
CS
U
TU
TI
TH
JY
DT
AZ
AU
TD
CK
BO
AK
VT
QX
O
CJ
sx
MA
AJ
UN
SD
K
PC
HP
It UK
x P
x ffl
x NJ
Above control limit
Below control limit

-------
50/50          EMSL-LV Performance Evaluation: Blind-B,  19-Apr-1994
Cesium-137

 % responding labs	     Frequency distribution
 10-
     -6            -4            -2            0            +2            +4           +6
                    . Normalized deviation of the mean from the known value


 % responding labs      	Frequency distribution


 10-
                                                    >••   T
     -6            -4            -20+2+4            +6
                    Normalized deviation of the mean from the grand average

-------