United States
           Environmental Protection
           Agency
           Office of Research and
           Development
           Washington, DC 20460
EPA 600/R-95/017B
February 1995
&EPA
Blind-B Performance
Evaluation Study

A Statistical Evaluation of
the October 18, 1994 Data
                                          0593RSD94COV-017B

-------
                 Blind-B
       Performance Evaluation Study
            October 18, 1994
      Environmental Protection Agency
Environmental Monitoring Systems Laboratory
            Las Vegas, Nevada

-------
            UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
                        OFFICE OF RESEARCH AND DEVELOPMENT
               ENVIRONMENTAL MONITORING SYSTEMS LABORATORY-LAS VEGAS
                                  P.O. BOX 93478
                            LAS VEGAS, NEVADA 89193-3478
                                   (702/798-2100)
Dear Participant,
   Enclosed are the results of the Nuclear Radiation Assessment Division (EMSL-LV)
Performance Evaluation Study for Blind-B; October 18, 1994.

   The known value for each analysis was determined by gravimetric methods,
checked by chemical analyses performed by EMSL-LV's Radiochemistry Laboratory,
and compared to the participating laboratories' grand average.

   The expected precision, determined by the known value, was taken from
"Table 3. Laboratory Precision:  One Standard Deviation Values and Control Limits
for Various Analyses", which is based on data accumulated over the years by the
Performance Evaluation Program, and can be found in the Environmental Radioactivity
Performance Evaluation Studies Program and Radioactive Standards Distribution
Program information brochure.
   Please take a few minutes to review this report and the analytical data your
laboratory submitted to us.  If there are any apparent discrepancies, please notify us
immediately.

   We encourage you to make use of the computer-automated data-entry system
that has been in place for some time now. As the number of participants increases,
and it becomes unrealistic for us to receive results by mail or FAX, the computer
system will be our only avenue for accepting data.

   If you have any questions or comments, please send a message via the data-entry
system or contact George Dilbeck at 702/798-2104 or Patricia Honsa at 702/798-2141 .
                                          Sincerely,
                                          George Dilbeck
                                          Chemist
                                          Radioanalysis Branch
Enclosure

-------
               NOTICE  .

This material has been funded wholly by
the U.S. Environmental Protection Agency.
It has been subject to the Agency's review,
and has been approved for publication as
an EPA document.

-------
               EMSL-LV Performance Evaluation: Blind-B,  18-Oct-1994             1/44


   The following pages consist of separate sections for each of the nuclides in this study with four
parts per section.  After the first, each part is separated from the next by a new page or a thick
horizontal bar.  The first page of each section is a statistical summary for the nuclide and starts
with a statement of the known value, the control limits, and the warning limits.

   The warning limits are placed at two normalized standard deviations above and below the
known value and the control limits are three normalized standard deviations above and below
the known value.  If you keep control charts, these values will be useful for anticipating problems
with the accuracy of your analytical methods.
   The coin shaped pie chart at the top of the summary page shows the fate of all the samples
sent out in number and percentage terms. The pie chart starts at the top and rotates clockwise.
The first sector represents those participants who submitted analytical results within both the
warning and control limits. The next sector represents those who are in the warning region but
not out of control. The third sector represents those who are out of control, but have passed
the outlier test. The fourth sector represents those who have failed the outlier test. The last
sector represents those participants who have failed to respond properly. This is the case if no
analytical results were returned, or less than three determinations were reported, or if the results
were received too late.  The reeding on the edge of the .coin is spaced at one percent intervals, and
the sector shading becomes darker as the data reliability decreases. Sectors with zero width are
not shown.
   The table in the center shows a number of statistical quantities calculated from the submitted
data based on the mean and median values in relation to the known value, both before and after
outlier removal. The lower pie chart uses the same construction as the upper chart and shows
the distribution of properly submitted data in terms of deviation from the known value divided
into sectors representing  one, two, three, and greater than three normalized standard deviations.

   The second part is an  alphabetical listing, in lab-code order, of submitted data and several
calculated quantities. An entry that is shaded has been rejected because of one of the reasons
listed above or failure of the  outlier test. The fifth and sixth columns are a measure of laboratory
precision. The Range analysis is a normalized value that you may use to keep precision control
charts. If this value is between 2.0 and 3.0,  your analytical process precision is in the warning
zone; if it exceeds 3.0 it is out of control. The eighth and ninth columns are the differences from
the mean of all non-outliers and from the known value, respectively. A tag symbol may appear in
the last column. Each page with tags has a  symbol definition summary at the bottom.  If there is
no tag symbol, the data is within the control limits, but it may be in the warning zone.

   The third part is a three-column listing of result average, tag symbol, and lab-code in average
order excluding those labs not responding properly. In this order, all outliers and out-of-control
results appear at the top  or bottom of the list.
   The last part is two bar chart displays showing frequency distributions of responding
participants. The first chart places the known value at the center and a bar at each 0.2 unit of
expected precision.  The second chart places the mean of the reported measurements at the center
and a bar at each 0.2 unit of standard deviation. In both cases,  a bar includes those results within
0.1 unit up to the maximum of six. Any results more than six units from the center value are
shown cumulatively by a shaded bar one past the sixth unit. If the central tendency of the known
value distribution falls away from the center, an error in accuracy is indicated. If the distribution
is broad, poor precision is indicated. The mean value distribution is similar but uses the average
and standard deviation of reported results as its basis.

-------
2/44            EMSL-LV Performance Evaluation: Blind-B,  18-Oct-1994


     The Range Analysis(R + SR) is calculated from the range, mean range and standard error of
  the range values.  The range is the difference between the maximum and minimum results for the
  laboratory. The mean range is calculated by multiplying the expected precision by 1.693(for three
  results).  The standard error of the range is calculated by multiplying the mean range by 2.575(for
  three results), subtracting the mean range from this product, and dividing the result by 3.  If the
  range is greater than the mean range, then the range analysis is calculated by subtracting the
  mean range from the range, dividing the result by the standard error of the range and adding 1.
  If the mean range is greater than or equal to the range, then the range analysis is calculated by
  dividing the range by the mean range.
     The normalized deviation of the mean from the grand average is calculated from the deviation
  of the mean from the grand average and the standard error of the mean values.  The deviation of
  the mean from the grand average is calculated by subtracting the grand average from the
  average of the laboratory's three results. The standard error of the mean is calculated by
  dividing the expected precision by the square root  of 3(the number of results). The normalized
  deviation of the mean from the grand average is calculated by dividing the deviation of the mean
  from the grand average by the standard error of the mean.
     The normalized deviation of the mean from the known value is calculated from the deviation of
  the mean from the known value and the standard  error of the mean values.  The deviation of the
  mean from the known value is calculated by subtracting the known value from the average of the
  laboratory's three results.  The standard error of the mean is calculated by dividing the expected
  precision by the square root of 3(the number of results). The normalized deviation of the mean
  from the known value is calculated by dividing the deviation of the mean from the known value by
  the standard error of the mean.
     A complete explanation of the statistical calculations involved in the report may be found in
  the Environmental Radioactivity Performance Evaluation Studies Program information brochure
  [Draft Revision of EPA-600/4-81-004], available from George Dilbeck, EMSL-LV, 702/798-2104.

-------
                 EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
                                   3/44
Gross Beta                          Statistical Summary                      193 Participants
The known value of this nuclide is 142.0 pCi/I with an expected precision of 21.0; the control limits
are 105.6 to 178.4; the warning regions are 105.6 to 117.7 and 166.3 to 178.4
44(22.8 %) Failed to respond •.
3(1.6 %) Outliers'
11 (5.7 %) Out of control'
      but not an outlier


        Statistic
                103(53.4 %) Within all limits
Respondents
- 32(16.6 %) In warning zone
           but within control


              Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
    127.49        Grand Avg 125.57
     41.94                     13.92
   1758.73                    193.70
     32.90                     11.08
    -10.22                    -11.57
     -0.35                     -1.18
    125.67                    125.67
    -11.50                    -11.50
     -0.39                     -1.17
14(9.4 %) More than 3 norm. S.D.
32(21.5 %) Between 2 and 3 norm. S.D. •
            . 45(30.2 %) Within 1 norm. S.D.
                           of known value

     58(38.9 %) Between 1 and 2 norm. S.D.

-------
4/44
EMSL-LV Performance Evaluation: Blind-B, 18-Oci>1994
Gross Beta
Lab
A
AE
AF
AH
At
AJ
AK
At
Res. 1
127.0
105.0
138.0
"'••:-', -r\\! v;-"

;:\; -v.';>>
120.0
141.0
Res. 2
132.0
115.0
128.0
ปV Cv-Sv'5'
**
;:.-'- -<':", "''..',
126.0
155.0
Res. 3
130.0
100.0
126.0
•>' *• "^ " "•• *.
v "• "' / "•
\ *f',\ v-l' ^
131.0
144.0
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
2.52
7.64
6.43
^x-;C^. * '.'

v' ':'f '-'-",,
5.51
7.37
0.141
0.422
0.338


1 "* '
0.309
0.394
129.67
106.67
130.67
j -.^ > * * *
" * • •
/ "" '*• '"'•' .>:
125.67
146.67
0.34
-1.56
0.42
\ ""•• "i^f i ^ '"J.
; "*,'-, ' 'x; '
.. ,.:f "T'V^;
0.01
1.74
-1.02
-2.91
:0.93
v-^f \^: -V^*-:
': ' ' ,<'••ป'> -'-;
• ;-% , •' - - * -;
^^'^•y '
-1.35
0.38
A&*"- '" **"'> :'ป-"••' ''-'A" '-": •.>''-* ;: -" ' ; >- '•' '"•"'•'.* : -"; - •'•' -~''" ' '": ', -' '•"
AP
AR
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO,
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
CS
CX
D
DB
DD
DE
DG
'DjK
DL
DM
123.0
139.0
154.0
127.0
116.0
128.0
123.0
'* - - i&O -;:
120.0
137.0
- ' ' * ". ,
130.0
127.0
131.0

144.0
124.0
128.0
123.0
120.0
135.0
• * ;. - , ~-\
115.0
126.0
116.0
124.0
109.0
137.0
157.0
131.0
133.0
117.0
'"• s '"•"•/
122.0
105.0
127.0
143.0
155.0
123.0
110.0
123.0
121.0
96.0
122.0
138.0
~, "-./'
133.0
130.0
134.0

146.0
122.0
133.0
123.0
120.0
141.0
\ s ^ , *s *,.
118.0
125.0
113.0
119.0
119.0
136.0
157.0
127.0
134.0
114.0
•• " -\" ""•- ,
122.0
106.0
129.0
141.0
157.0
125.0
108.0
127.0
124.0
&8.0 ,
123.0
130.0
'- --> ,- ' - , \<
135.0
132.0
136.0

147.0
128.0
126.0
121.0
120.0
143.0
'il-:;:^'^-""
105.0
128.0
114.0
114.0
117.0
138.0
153.0
123.0
135,0
116.0

121.0
106.0
• s No data submitted
0 =
Insufficient
data
X s
3.06
2.00
1.53
2.00
4.16
2.65
1.53
47.3S
1.53
4.36

2.52
2.52
2.52

1.53
3.06
3.61
1.15
0.00
4.16
f':'\
6.81
1.53
1.53
5.00
5.29
1.00
2.31
4.00
1.00
1.53
'
0.58
0.58
0.169
0.113
0.084
0.113
0.225
0.141
0.084
3.542
0.084
0.225
-•
0.141
0.141
0.141

0.084
0.169
0.197
0.056
0.000
0.225

0.366
0.084
0.084
0.281
0.281
0.056
0.113
0.225
0.056
0.084

0.028
0.028
126.33
141.00
155.33
125.00
111.33
126.00
. 122.67
121.67
135.00

132.67
129.67
133.67

145.67
124.67
129.00
122.33
120.00
139.67
''. ?"'
112.67
126.33
114.33
119.00
115.00
137.00
155.67
127.00
134.00
115.67
. .. ._.
121.67
105.67
TAG SYMBOLS
Determined
to be an
outlier
0.06
1.27
2.45
-0.05
-1.17
0.04
-0.24
-- -4v61 -':v™-
-0.32
0.78
,^- ,'v x-'1:;-
0.59
0.34
0.67

1.66
-0.07
0.28
-0.27
-0.46
1.16
*•/<•' ''A & :'VS_
-1.06
0.06
-0.93
-0.54
-0.87
0.94
2.48
0.12
0.70
-0.82
. ''', ,,.C,, ^' ^ ,'' A ..;.. /
-0.32
-1.64
ft = Above
•li s Below
-1.29
-0.08
1.10
-1.40
-2.53
-1.32
-1.59
-$#7 X
-1.68
-0.58
;*;J-(- \ >V*;
-0.77
-1.02
-0.69
- %'',- ' • /
0.30
-1.43
-1.07
-1.62
-1.81
-0.19
L-_V >-s-'-ซt/'
-2.42
-1.29
-2.28
-1.90
-2.23
-0.41
1.13
-1.24
-0.66
-2.17
~*"^',\ ",; ~\ '
-1.68
-3.00
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
5/44 ]
Gross Beta

Lab
DO
DS
DT
DZ
E
EB
EL"
EO

ER
EV
FF
FJ
FL
FN
FU
FZ
GE
GI
GQ
GT
GZ
HI
HK
HL

HP
HX
I
1C
ro
IE
J
JE

JG
JN
JQ
JS

JX
JY
K
-..'iCB!

KT
KX
L
LF

Res. 1
';v'-;t^:\--va
I ' •' fJ-" ••> x-
136.0
120.0
127.0
134.0

135.0


123.0
3.0
120.0
113.0
88.0
105.0
100.0
121.0
X
129.0
31.0
598,0
120.0
125.0
137.0

114.0
I;
129.0
115.0
117.0
118.0
120.0
137.0


118.0
156.0
112.0

, .
118.0
104.0
- - -t-"
\
140.0
140.0
144.0
130.0

Res. 2
\ ;•<•;;'-//:
:;rV^H^
135.0
110.0
127.0
134.0
-T'^y ~ v
136.0

, ',ซ••; > -- •'
124.0
'"-. io
105.0
113.0
84.0
104.0
95.0
122.0
v ^ >*
118.0
* ' 30$
586.0
120.0
127.0
138.0

118.0

123.0
119.0
111.0
108.0
121.0
137.0

s
107.0
165.0
116.0
\ \

117.0
99.0
! *• V , % ' - *

145.0
142.0
145.0
130.0

Res. 3
, •>* ^ * *
S::V^v'?> ^
144.0
116.0
127.0
137.0
-.v...'''"''' *!"• v'v \
137.0

' ;'V - : - >~\ ฐ
126.0
4.0
110.0
109.0
81.0
101.0
120.0
122.0
v xi *
124.0
." s -^ - _ <.
x 684.0
120.0
129.0
137.0
1
114.0

132.0
118.0
111.0
121.0
118.0
140.0


116.0
160.0
125.0


115.0
99.0
s ?* V^ *
-.-• " -. %
150.0
137.0
145.0
120.0
• s No data submitted
0 a
Insufficient
data
x =
Exper.
Sigma
- .

4.93
5.03
0.00
1.73

1.00


1.53
0.58
7.64
2.31
3.51
2.08
13.23
0.58

5.51
x
7.81
0.00
2.00
0.58

2.31

4.58
2.08
3.46
6.81
1.53
1.73


5.86
4.51
6.66


1.53
2.89

V
5.00
2.52
0.58
5.77
Rnganal
(R + SR)

.- xX'
0.253
0.281
0.000
0.084

0.056


0.084
0.028
0.422
0.113
0.197
0.113
0.703
0.028

0.309

0.394
0.000
0.113
0.028

0.113

0.253
0.113
0.169
0.366
0.084
0.084


0.309
0.253
0.366


0.084
0.141


0.281
0.141
0.028
0.281
Normalized deviation
Average
1 ,.*3" S; ''-::
- \v -V;^vy.
138.33
115.33
127.00
135.00
- , ; - "v ! ,,
136.00

~- ••• - ' •^
124.33
3;67
111.67
111.67
84.33
103.33
105.00
121.67
s
123.67
sx ,
589.00
120.00
127.00
137.33

115.33

128.00
117.33
113.00
115.67
119.67
138.00


113.67
160.33
117.67

,
116.67
100.67

X\ V.
145.00
139.67
144.67
126.67
TAG SYMBOLS
Determined
to be an outlier
(grand- avg) (known) Tag
^^•-vV^V-
^-'xf!*^' ^;
1.05
-0.84
0.12
0.78
'-^r^c"-^ ^^
0.86

^->"\ ,:••' !',-:'.-s '•'
-0.10
; .10*05
-1.15
-1.15
-3.40
-1.83
-1.70
-0.32
v x
-0.16
^.-N
v 38.22 x
-0.46
0.12
0.97

-0.84

0.20
-0.68
-1.04
-0.82
-0.49
1.03

0\;>\:f v ,,, ' ":,• "
'^-v---: > %-.
-0.30
-2.20
-1.24
-0.58
;:"-v\:- >: ."-
-0.49

N > - ' ' > - *
-1.46
11.41 x
-2.50
-2.50
-4.76 U
-3.19 $
-3.05 U
-1.68
ซ-
-1.51
" s "^ 0
36.87 x
-1.81
-1.24
-0.38

-2.20
•
-1.15
-2.03
-2.39
-2.17
-1.84
-0.33

-t"\- -- _ \ •-
-2.34
1.51
-2.01

•
-2.09
-3.41 11
" v „ • , - , *

0.25
-0.19
0.22
-1.26
control limit
control limit

-------
6/44
Gross Beta
Lab Res. 1
Id
LL
LR
LT
M
MA
MP
MQ
MV
MY
Jjf V
NA
NH
NJ
NK
NO
NT
0
OF
OS
OX
OY
P
PA
PB
PG
Pi;:
PM
PQ
PR
PV
PW
Q
QC
QJ
QP
QQ
QT
QU
QW
QX
QZ
HC
RD
• =
0 s
;/ "• ' ^ $^,T'-,, !,-'
119.0
131.0
110.0
110.0
116.0
"""'•i^*'' I '•"^ifY
132.0
143.0
122.0
'•^"':; P'.;
154.0
124.0
137.0
131.0
123.0
132.0
128.0
125.0
153.0
118.0
112.0
122.0
125.0
144.0
131.0
" >. "; "• "
' -'f '•'•:
126.0
135.0
98.0
115.0
140.0
143.0
114.0
121.0
98.0
123.0
141.0
114.0
127.0
^
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Res. 2
•^V$/-*ปy
118.0
140.0
110.0
108.0
117.0
r^T''v*~7i:ฃ
103.0
152.0
124.0
Cv^?&>;'
150.0
118.0
123.0
126.0
125.0
133.0
124.0
124.0
155.0
121.0
117.0
122.0
122.0
145.0
136.0
::;-\'VV '';':
133.0
136.0
94.0
114.0
V1- '"* -. '
152.0
143.0

125.0
127.0
120.0
120.0
142.0
116.0
120.0
.' - .x,> - "*'''' '-
Res. 3
.-•>. ^>y
119.0
126.0
114.0
110.0
120.0
''' -. s * *
138.0
135.0
122.0
ST> -3':r
156.0
90.0
129.0
135.0
127.0
133.0
117.0
123.0
155.0
124.0
113.0
120.0
124.0
142.0
123.0
-^.\-'~ ':' "'
122.0
140.0
94.0
117.0
153.0
144.0
120.0
131.0
. 125.0
118.0
144.0
120.0
127.0
*y ^ * - ' r
No data submitted
Insufficient
data
X =
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
<<•*•;** '"'
0.58
7.09
2.31
1.15
2.08

18.72
8.50
1.15
' T - >-'•:
3.06
18.15
7.02
4.51
2.00
0.58
5.57
1.00
1.15
3.00
2.65
1.15
1.53
1.53
6.56
',: , /v
5.57
2.65
2.31
1.53
7.23
0.58
f '"• f
5.51
5.03
14.36
2.52
1.53
3.06
4.04

0.028
0.394
0.113
0.056
0.113

0.984
0.478
0.056
*v-:
0.169
0.956
0.394
0.253
0.113
0.028
0.309
0.056
0.056
0.169
0.141
0.056
0.084
0-084
0.366

0.309
0.141
0.113
0.084
0.366
0.028
0.309
0.281
0.759
0.141
0.084
0.169
0.197
/' 	 /,' v\<;
118.67
132.33
111.33
109.33
117.67
;^ ,vv. v. ^f
124.33
143.33
122.67
• %;%;;,
-0.57
0.56
-1.17
-1.34
-0.65
* V*;: <**;'*•
1.92
-0.80
-2.53
-2.69
-2.01
^ vซ y vffff,ff^e ^ v *vi-\f '••, •••••• f >"."' ffff ' vf Jv^fff-w^
-0.10
1.47
-0.24
v/f;'^:
2.29
-1.23
0.34
0.42
-0.05
0.59
-0.21
-0.13
2.37
-0.38
-0.95
-0.35
-0.16
1.49
0.37
'-':"'-, \.; ;:M
0.12
0.94
-2.49
-0.84
•<•;• / ,' ,-.
1.88
1.47
-0.49
0.06
-0.93
-0.43
1.38
-0.73
" J ^" "" •, ' w "''
'*, ' s *• I1" ** •? H
-0.07
tt = Above
U s Below
-1.46
0.11
-1.59
v"\< '^V'VV
0.93
-2.58
-1.02
-0.93
-1.40
-0.77
-1.57
-1.48
1.02
-1.73
-2.31
-1.70
-1.51
0.14
-0.99
^^V"'" ''**•";
-1.24
-0.41
-3.85 11
-2.20
0.52
0.11
-1.84
-1.29
-2.28
-1.79
0.03
-2.09
•-' s /\*"" '> "V"' \ ' '
' '"-- " C"v '* •^"-\;
-1.43
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
7
/44 ]
Gross Beta

Lab
RF
RG
RJ
RK
RL
RM

RP
RR
RV
RZ
S
sc
SD
SF
SI
SL
SM
SN
SO
SR
ss
ST
SW
sx
sz
T
TO
TE
TH
TI
TL
TN
TQ
TS
TY
U
UA
UE
UG
UK
UN
UP
UQ
uw
UY

Res. 1
: . :i,^flr - -s
115.0
132.0
102.0
* ~~ ; '\ Vv'"V
143.0

\r //''W^
x, s- •-
151.0
108.0
135.0
128.0
120.0
150.0
84.0
125.0
115.0
105.0
133.0
115.0
117.0
134.0
, j,Y- ,
149.0
123.0
127.0
139.0

138.0
99.0
131.0
139.0
123.0
142.0
115.0
133.0
129.0
156.0


87.0
122.0
126.0
135.0
128.0

Res. 2
" i -s\, v* i %%"
120.0
136.0
102.0
- \-; t--"
135.0

\- \\C>v;^,-
; C -• >'•- %
173.0
108.0
143.0
114.0
111.0
145.0
99.0
122.0
102.0
101.0
133.0
122.0
125.0
122.0
", ;V^%:'"
141.0
126.0
127.0
123.0
v
142.0
105.0
128.0
128.0
139.0
147.0
115.0
126.0
128.0
149.0
- ' ,
'\ "'' ''
118.0
128.0
132.0
128.0
126.0

Res. 3
ฐs \ s V X\ ••
118.0
134.0
103.0
1A-\>T'r;v' ' ;
137.0

S'P^'r
x •
167.0
112.0
139.0
128.0
105.0
144.0
93.0
130.0
123.0
96.0
130.0
108.0
112.0
125.0
V.^T,- "~ฃ-\
146.0
128.0
127.0
142.0

136.0
112.0
127.0
126.0
110.0
139.0
110.0
125.0
126.0
151.0

-
94.0
139.0
134.0
127.0
117.0
• 3 No data submitted
0 =
Insufficient
data
x =
Exper.
Sigma

2.52
2.00
0.58

4.16



11.37
2.31
4.00
8.08
7.55
3.21
7.55
4.04
10.60
4.51 .
1.73
7.00
6.56
6.24

4.04
2.52
0.00
10.21

3.06
6.51
2.08
7.00
14.53
4.04
2.89
4.36
1.53
3.61

^
16.26
8.62
4.16
4.36
5.86
Rng anal
(R + SR)
* - - '
0.141
0.113
0.028

0.225
v s •• - \ ••


0.619
0.113
0.225
0.394
0.422
0.169
0.422
0.225
0.591
0.253
0.084
0.394
0.366
0.338

0.225
0.141
0.000
0.534

0.169
0.366
0.113
0.366
0.816
0.225
0.141
0.225
0.084
0.197


0.872
0.478
0.225
0.225
0.309
Normalized deviation
Average
> ^ - ,'>'V-\;<
117.67
134.00
102.33_
"~ ;v'v!V*'X^
138.33

;:- :'-7;>:!;^

163.67
109.33
139.00
123.33
112.00
146.33
92.00
125.67
113.33
100.67
132.00
115.00
118.00
127.00
• Y-v^'H
145.33
125.67
127.00
134.67
% ^ •• - •>
138.67
105.33
128.67
131.00
124.00
142.67
113.33
128.00
127.67
152.00

" -
99.67
129.67
130.67
130.00
123.67
TAG SYMBOLS
Determined
to be an outlier
(grand-avg) (known)
^vซt->,-o,vf
• • " , • ' • ' c
3.14
-1.34
1.11
-0.18
-1.12
1.71
-2.77
0.01
-1.01
-2.05
0.53
-0.87
-0.62
	 0.12 	
-.rr^ry-'::-^^
1.63
0.01
0.12
•*'f>X;*
-2.01
-0.66
:3;2,L,-
%^:?;
-0.30



1.79
-2.69
-0.25
-1.54
-2.47
0.36
-4.12
-1.35
-2.36
-3.41
-0.82
-2.23
-1.98
-1.24
2 , v " " s ;
0.27
-1.35
-1.24
Tag
,-. • - -


11
:>"ฐ


'-'-9 .
• - ,






li


11




"Vซ.



0.75 -0.60
i,\.^ ^ ^^^ % •-" " ^ "WV^ ••_ AS Xsw X"%s ', ^ *
1.08
-1.67
0.26
0.45
-0.13
1.41
-1.01
0.20
0.17
2.18
>
* f.
-2.14
0.34
0.42
0.37
-0.16
tt s Above
& = Below
-0.27
-3.02
-1.10
-0.91
-1.48
0.05
-2.36
-1.15
-1.18
0.82

-.
-3.49
-1.02
-0.93
-0.99
-1.51
control
control

Ji








•
•
11




limit
limit
	 — -f

-------
8/44 EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Gross Beta
Lab Res. 1 Res. 2
VtH <.i..;\y?f ^^ff^K ''
VG 95.0 98.0
VI •>•,..:•',•,-.ซ r..'^.V-
VJ 108.0 111.0
^-i -./,;;:' ;''fi-:\V>l,
VO 134.0 139.0
VQ '". /--:'Vv *?'.
VT 147.0 132.0
vu ^,,. .>: , , /;,; ,>'
V •. "" ^* ' t X ••••', ** w ' **
* VX'*, ;"' "yV"-' '".--. •>," "->:
W 128.0 126.0
X 128.0 135.0

Exper. Rng anal
Res. 3 Sigma (R + SR)
>'-^A-K;'-?vC'.,' -" ':•'-/ ' ~;",< x^--
100.0 2.52 0.141
116.0 4.04 0.225
&'\?r^: .;\:; •'-•';'.•; : /' ^ •
137.0 2.52 0.141
-;-^'-;; •, '-'':",V-' • --; • -.'•/-"' ,-r
128.0 10.02 0.534
V !-: '^, , ; ; ' \ ,*- • , .,
'l^ /''' "" %^^ i * Ml> ''-.,'' S '
-' t'h V . /'> -:" ','-,- - , ^ , ••_ v ,
130.0 2.00 0.113
128.0 4.04 0.197
N
Normalized deviation
Average (grand-avg) (known)
:•,'•',-:'.';* ^J'';-'^'"'"*?^4*^^!Cป^
97.67 -2.30 -3.66
111.67 -L15 -2.50
ฐ ; :/\ , ' i \-:', :ซ-;,- ;T ''-^; ^ '*('- O'":/ '
136.67 0.92 -0.44
'--.;ป, ^.'V-;^*'','*'".'',-/:;;^'./;"',
135.67 0.83 -0.52
\ , - '-j- „ .'. ~~ , ''/, >''<". '
' > ' ' ~* : ' t^\ ' \V> f. * ^ V ' "' '' ' ,
•;•,.. -- ,-,,,;. '. s '/-.' •;,';"•>;••••;•• ,' -. "-" "". "
128.00 0.20 -1.15
130.33 0.39 -0.96


Tag
^;:'ปv!c
1,
;ฃซฃ,•:
:";*\;;:;

9-,

; • ,-

" • ' •'


Data sorted by Laboratory Average
Average Tag
3.67 x
69.67 x
84.33 U
92.00 11
95.33 11
97.67 U
99.67 U
100.67 11
100.67 U
102.33 11
103.33 11
105.00 Jl
105.33 11
105.67
106.67
109.33
109.33
110.67
111.33
111.33
111.67
111.67
111.67
112.00
112.67
113.00
113.33
113.33
113.67
• = No data submitted
0 = Insufficient data
Lab Average Tag
FF 114.00
BG 114.33
FN 114.33
SI 115.00
PR 115.00
VG 115.33
UN 115.33
SN 115.33
K 115.67
RK 115.67
FU 116.67
FZ 116.67
TI 117.33
DM 117.67
AE 117.67
RZ 117.67
M 118.00
NH 118.67
LT 119.00
AZ 119.67
VJ 119.67
FL 120.00
FJ 120.00
SD 120.33
CO 121.00
DD 121.33
TY 121.67
SM 121.67
JN 121.67
TAG SYMBOLS
Lab Average Tag
OY 122.33
QU 122.67
CQ 122.67
SR 123.00
CX 123.33
PV 123.67
HP 123.67
DZ 123.67
D3 124.00
DG 124.00
QZ 124.33
JY 124.33
1C 124.67
RG 124.67
MA 125.00
JS 125.00
SS 125.67
LL 125.67
CS 125.67
QQ 126.00
J 126.33
HI 126.33
CJ 126.33
QW 126.67
OX 127.00
P 127.00
GE 127.00
DL 127.00
BH 127.00
ft = Above control
x s Determined to be an outlier 11 = Below control
Lab
CG
MY
BC
O
sc
UY
PA
GQ
TQ
OF
MQ
EV
RD
CA
NO
AW
SZ
SL
AK
BA
QT
CP
AP
LF
T
ST
PM
HK
E
limit
limit

-------
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Gross Beta

Average Tag
127.00
127.67
128.00
128.00
128.00
128.67
129.00
129.67
129.67
129.67
129.67
130.00
130.00
130.33
130.67
130.67
130.67
131.00
132.00
132.33

% responding labs

Data sorted by Laboratory Average
Lab
DD
UA
W
u
I
TL
CE
UP
NJ
BN
A
UW
PG
X
UQ
NK
AF
TN
SO
LR

Average Tag Lab
132.67 NT
132.67 BM
133.67 BS
134.00 RJ
134.00 DE
134.67 TD
135.00 EB
135.00 BK
135.67 VT
136.00 EO
136.67 VO
137.00 PQ
137.00 D
137.33 HL
138.00 JE
138.33 RM
138.33 DT
138.67 TH
139.00 S
139.67 KX
139.67 CK
Average Tag
141.00
142.33
142.67
143.33
143.33
143.67
144.67
145.00
145.33
145.67
146.33
146.67
148.33
152.00
153.33
154.33
155.33
155.67
160.33
163.67
589.00 x
Frequency distribution
9/44


Lab
AR
QX
TS
QC
MV
PB
L
KT
sx
c
SF
AL
Q
UE
NA
OS
AU
DB
JQ
RV
GZ




ฐ 5 ' -4

% responding labs
10' -----------

ฐ -6 ' -4

• = No data submitted
0 = Insufficient data
• ••••ill •
... lillllllLil.j. . __
-2 0 +2 +4
Normalized deviation of the mean from the known value
Frequency distribution
.• lllll .
_ _ .-..-•.Illmllllll 	 _ _
-2 0 +2 +4
Normalized deviation of the mean from the grand average
TAG SYMBOLS It = Above
x = Determined to be an outlier JJ = Below


+6




+6

control limit
control limit

-------
                  EMSL-LV Performance Evaluation: Blind-B,  18-Oct-1994
                                  10/44
Strontium-89                       Statistical Summary                      193 Participants
The known value of this nuclide is 25.0 pCi/1 with an expected precision of 5.0; the control limits
are 16.3 to 33.7; the warning regions are 16.3 to 19.2 and 30.8 to 33.7
116(60.1 %) Failed to respond •
3(1.6%) Outliers
4(2.1 %) Out of control	
     but not an outlier


         Statistic
                . 63(32.6 %) Within all limits
Respondents
*• 7(3.6 %) In warning zone
         but within control


            Non-outliers

Mean
Std. Dev.
Variance
% Coef. of Var.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
     23.72
      5.53
     30.58
     23.31
     -5.13
     -0.23
     22.67
     -9.33
     -0.42

  Grand Avg 22.99
               4.16
              17.27
              18.08
              -8.05
              -0.48
              22.67
              -9.33
              -0.56
8(10.4 %) More than 3 norm. S.D. •ป
6(7.8 %) Between 2 and 3 norm. S.D. *
              2(41.6 %) Within 1 norm. S.D.
                           of known value
     31 (4O.3 %) Between 1 and 2 norm. S.D.

-------
11 /
44
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994

Strontium-89
Lab
A
AE
AT
AH
,-AI.-
" AU-;;
AK
AL
AO
AP
AB
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
CS
CX
D
DB
DD
DE
DG
pjr
DL
DM
Res. 1
23.0
23.0
27.0

e-/:"V'.\,>\\;
' *',.:[* ;'•> ''•,,
24.0
27.0
v "!. -. •• , J
25.0
18.0
25.0
29.0
21.0
< •-" ' f
23.0

23.0
22.0
30.0
30.0
20.0

32.0
27.0
42.0

** ' *<\
, " \ ~ "x.
23.0
23.0
27.0


24.0
23.0
8.0

.Wn:,
Res. 2 Res. 3
23.0
23.0
28.0
'--s -/_'•: '-ซ. ,\
>\-.s' •• "• •• ฐ "x
-'">!':A >?'/>- y**":\
25.0
29.0
'>V ^'^.{.vC
24.0
20.0
28.0
32.0
20.0
,'V -" -;/> - -\>--;
23.0

26.0
25.0
28.0
' ^ \
29.0
21.0
% ' -. ^ ' <.""•-
25.0
24.0
'" 39ปp-y,:,,
s. v ;W^/%^
,\ .i^%$?Mv^
r:'^!'1^:''^^
20.0
22.0
24.0
s <•. <• ?
. '•'•;- • * ••- ,-
21.0
23.0
13.0
'"* ,• -' . - ; r
""" "" ' ^ ~~ vVv -.^ ' "*
23.0
22.0
25.0


=,'v\^'-'
24.0
29.0

1 ?''*-* -
27.0
21.0
26.0
27.0
20.0
""•'- "k
24.0

17.0
21.0
31.0

28.0
21.0

29.0
23.0
41.61
,;>:?-:'
l>ln^}'
!/"/.,;;!' ;
20.0
22.0
27.0

, , * V
20.0
23.0
12.0

S ""s '•- V "" ^^
:v- V,;;, >j
• s No data submitted
0 =
Insufficient
data
X 3
Exper.
Sigma
0.00
0.58
1.53
- , -
;0 •;ซ•"'. . ^
V * - - ' x
0.58
1.15


1.53
1.53
1.53
2.52
0.58

0.58

4.58
2.08
1.53
1.00
0.58

3.51
2.08
i.83
-'• ' •' ,
--,* "v \" ': " ' ' *

1.73
0.58
1.73


2.08
0.00
2.65

•• -' / , ' ' '• s
Rnganal
(R + SR) Average
0.000
0.118
0.354



0.118
0.236

0.354
0.354
0.354
0.591
0.118

0.118

1.120
0.473
0.354
0.236
0.118

0.827
0.473
0.354



0.354
0.118
0.354


0.473
0.000
0.591

,' \-- -
23.00
22.67
26.67


" /. '-'••; * ' ^ V
24.33
28.33
"•' \Z' " " ••
25.33
19.67
26.33
29.33
. 20.33

23.33

22.00
22.67
29.67

29.00
20.67
J
28.67
24.67
40.67

- _ - - -c^ -
,.,,": •
21.00
22.33
26.00

'* -. "•
21.67
23.00
11.00

~l "' "•,,• *'*
TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known) Tag
0.00
-0.11
1.27
v'\ /-•
/ ' ,*• > ^ ' ' ' -X
•;' ^,.\-%/ ^'^-r-
0.47
1.85
'•''-s-v'' ' 1S - ,.>••>•
0.81
-1.15
1.16
2.20
-0.92
'"" '' ( v 'V """
0.12

-0.34
-0.11
•• , l , "; ~ ; ;-'•.'
2.31
*" *• f ? "• "" '
2.08
-0.80
" " ':',-'" , '
1.97
0.58
""'6.1& - ';-
-';•• : '' -'-'-"'^V "•'••;
'-' > ' - -'"•?-' -,-'-1
:- , ' / --,"* '- •;;
-0.69
-0.23
1.04
"H ; - ' '' " '
-'•' -: •"'- ; ' ~"
-0.46
0.00
-4.15
\ '*' ">;i'X
s ""' ' •. / •" ' J~~
' •• "" - ' >. ^ v "5 *j
11 s Above
U- s Below
-0.69
-0.81
0.58
'- . ;^;!; :'•;'"'• -
ป,.;>; *;V>~i
.r'txp-" 'i,:-'(
-0.23
1.15
>' ^ '• • •--
- , -> • - ,
-; >.- :\. •'••'• -
0.12
-1.85
0.46
1.50
-1.62
^VV-V-,";*-
-0.58
*' '
-1.04
-0.81
; '**•" '•;•'
1.62
" '-. : 'f
1.39
-1.50
'"•;.?'• ••",'•• *
1.27
-0.12
'.'&v43'' " x\
T" *'.
."'^v:''!^*v"
control limit
control limit

-------

EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Strontium-89
Lab
DO
DT
DZ
E
EB
EL
EO
ER

EV

Wfjjf


FF

FJ

FL\
•FIT
FU
Res. 1
25.0
24.0
22.0
14.0
37.0
19.0
>;• - *
L^tl^Vx'"1

S\tVv-s> L~, "' -' 'V
' * -.^ -' * -* *,
N^ * *x"- % -; v \


- ^ -^ \,-*' '• •>

!*„ -0 ซ,,~

C>V ' "!- ."-' I'--
\^"v^--;!; ;7
33.0
Res. 2
	 25.0
26.0
21.0
14.0
26.0
21.0
"".^o'^KT,
V^': ^

-. ! \>V ;5 4Lฅ""'
- v^ ^ ,,\X-- y^-.'
x.v ^ x^x^^ ''^


' ^ ! - -"-/^"\

" " " ' -, xV
i-- -. , ; ^ ^ ^
^X, ,, ^ •.^""•% s^ \
V?y -,y;\;;-
28.0
"F2f ?" " .JTT-"? "vT^^'.HY

GE
GI
GQ
GT

GZ
ffl
HK
HL
HP
HX
I
1C

m
IE
J
JE
JG
JN

JQ
JS
JX
JY
K
KB
KT
KX
L
;LF\
• =
0 s
, * v "•"••• "."Vy " ""^ -. ^
, ^ ,->"-':„; v *'••„,
>~.o^\,x ., ;,_,_
23.0^^
;i*")\-' v*\ ."ฃ*;*

,s;"~ •' ^-\'s-" •-".
• ~ ,<' ^ >• .'
23.0

22.0

27.0
24.0

•."-,'"•
x. - -\' " \ ' "
20.0
20.0
' "-X ' ,-'"-*,^-
*x -• \ v, ,

s-
25.0

14.0
19.0
'. ,:'„ , \;\,
'--•>-' ,,-
19.0
26.0
.v^>!l'3
N^-.* x\ s ^->\l'1 ^O^^
C^iX>^'^-
K^C^^St:
24.0
^-^S*~ Xfv'

C\, ^vxV/ ~
^ V > -\-;--; 7
22.0

19.0

29.0
22.0

*"" \ \> ~-' "!-X
y: ' ~v^lr
19.0
16.0
^'W'^.'f-C^V'-1 Cs
,!'-" -"4^-f ; •'%,
-, ^H s ^ X ^ V ^ ^
s
24.0
< " -
18.0
15.0
Y'-'",* ' > "" :-?-\s
-V;$-\^
21.0
26.0
-^'vlrj^^
Res. 3
18.0
24.0
21.0
15.0
28.0
17.0
\
" ; *' -''*"-.",-

x-,,iN-Xi •*
* •• \ \ *
<• "• -.s' , ^ ;, ;


- ".ซ,- .

"'_,/'

- t'*v :
^ " s v
31.0
V"!1;",
S ^ s1"1^ i\ ''
^•j\v^ ;-
:<- "*" ••'
25.0
ซ"* 0 <_ ^ s ^ i ..


•" *"*••• *''
22.0

19.0

32.0
25.0

;; '/ *-:._
Y,\--;--
18.0
15.0
,^?-)-:rr ~



24.0

13.0
25.0
-^ _.•• " v
> \',:'-;;
23.0
27.0
-'~Y'i)?,'\r'v
No data submitted
Insufficient
data
X s
Exper.
12/44
Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
4.04
1.15
0.58
0.58
5.86
2.00

^

0 -






\



2.52
, " ' !

s \ ""
- - ''
1.00




0.58

1.73
v.;>;;'.-'V!'
2.52
1.53

" , t -
A • /
1.00
2.65

^


0.58

2.65
5.03
v

2.00
0.58

0.827
0.236
0.118
0.118
1.570
0.473

"' •'•?''

-' V - 'ป"




^



v

0.591


~ •••• ^c ' s •
"• % \X
0.236




0.118

0.354

0.591
0.354



0.236
0.591
% %



0.118

0.591
1.345


0.473
0.118
, „ , • ,
22.67
24.67
21.33
14.33
30.33
19.00
" - " x;-'^---" -""" "\x
i " •- v" {••<•. \V --\\ V-."X^ ^

^^ A ?^ aX "" ^ ^ ^ ^ ^^
•\__ \ "; * ^ , ^ "-Vx" ^
Xx % o ^ ^^ ^ Y-. %i^'"lSi:'sS'*


- ^" - ,\;^i^\x-^

•• "-.'"X^ Si_ \ "-^

% ; ' , \ ^'x ,~ s
- ^ " ^-'i
30.67
-ft-; ; A-. '' ; •• ฐ ^ •••• V^X\' "> " *" Xx --v sf
•c7^v-x^V?;ri^V;}-
'Y;?^^^!^:^
24.00
• \ <\ - - • <"-x\x V~' ' ;

'"'' -^ 'i".'\v;'o
- • >: \ 'v-;:i -
22.33
x{ "'U
20.00
,V -x - -
29.33
23.67

', "-'\! ,,! V,
- --• \- c--;\; ,ปr-
19.00
_ _m17.00^ 	
V- \---$™t;v*?f"?5^
, .'• T> , -,x";


24.33

15.00
19.67
;lrfV;,v^*Vk
<•'"'' *" •• i*" '"• *• % ''
21.00
26.33
' •"' "^i'^-y
TAG SYMBOLS
Determined
to be an
outlier
_-q.ii_ 	
0.58
-0.57
-3.00
2.55
-1.38
Ll's \ : ^ ,^}r->'
"iK'"-x ^V)V

\j, -^ *• ••V-vf-'VJ*?'
-s 'X'" C - ^ , ,"^>
- % x^ N, s • \ ^-•.^ ,


-\'x"'-^ " ;^' V*X''-

4.X *' • , Y > -!

"h> i"-:'^\3x
rv y'; : ^>i? i;"-;ฐ:
^ 7,2.66..','_
rf^;\^x<,-";tV- r;;j
4-\ , " " X N ^ s.X
'^v/i-ijHx^
f/f;^;c;ti
_^q.35j^ ^_
^A"",":;"-,'7- \!

S" !T~-S'- - ',;-'
"" •• "" •• •> '\ \?
-0.23

-1.03
' -" ? - v'c
2.20
0.24

>-l,'"';';v%;>\s? --;
^vx;'^:;^^
-1.38
_-^07^ 	
,^^TXt^
'' -^


0.47

-2.77
-1.15
;;:f;;?'\w'Y-*'
v;^:'^ :'*:'\ , -
-0.69
1.16
v^^:':^
ft s Above
11 = Below
-0.81
-0.12
-1.27
-3.70 li
1.85
-2.08
Mxf ""'' •""
tf.VxV- :ซ

\V*^f-- • s
XN /- * ^ >,'
J, -• X. * x * *


svi;^ "• *

" K> - •

\xf::\!V ••
*' * '<"''"''':•, • '
1.96
>^V^ VV-0
\' •* v-- -
%*^*Vt x *
Xซ v" ' i S1 ^ ' '
-0.35
x >•"' >'. , J *
" -\ •• X "" v v
" >•• "" *
*i v s •
-0.92
o" ! ' • f V •
-1.73
,- -- - ,..•••••
1.50
-0.46

* i,\\-V" :\.?- -
:|^;Aflป>
-2.08
_:2.77 	
i^%%~V •
;i'r'-v ' ', ~ •

~ " *
-0.23
•
-3.46 JJ.
-1.85
VY-^ ,-^ •
h;: ">:- " •
-1.39
0.46
•-.. * ; "'•,''-''
control limit
control limit

-------
 13/44
                 EMSL-LV Performance Evaluation:  Blind-B, 18-Oct-1994
Strontium-89
                                       Exper.   Rng anal
Lab     Res. 1     Res. 2      Res. 3     Sigma   (R + SR)   Average
                                                                      Normalized deviation
                                                                      (grand-avg) (known) Tag
 LR
 LT
 M
 MA
 MP
 MQ
21.0
22.0
          22.0
          25.0
          \ ;,v   ff
                              21.0
                              23.0
                               0.58
                               1.53
.,':  *• x\; /;JK vW'^-i,; It?,.' ;-"•-  -->///
24.0      21.0       22.0      1.53
 MY
-N,
 NA
 NH
 NJ
 NO
 NT
 O
 OF"
 OS
 OX,
 O Y
 P
 PA
 PB
 PO
 PI
 PM
 PQ
 PR
'PW-
 Q
 QC
 QJ
 QP
 QQ
 QT
 QU
 QW
 QX
 QZ
"BC"
21.0      26.0       22.0      2.65
17.0
26.0
25.0
26.0
22.0
20.0

27.0
                    20.0
                    27.0
                     23.0
                     27.0
                               3.00
                               0.58
                    25.0
                     25.0
                               0.00
                    21.0
                     29.0
                               4.04
                    21.0
                    20.0

                    29.0
                     19.0
                     18.0

                     25.0
                               1.53
                               1.15

                               2.00
0.118
0.354
                                                  0.354
0.591

0.709
0.118
0.000
0.945
0.354
0.236

0.473
                                                    21.33
                                                    23.33
                                                    22.33
                                                               -0.57      -1.27
                                                                0.12      -0.58
                                                               1  V- .-'SV'*^-'''  -' v^^ V
                                                                            ,- /^ v'\;-,,;- vr->>
                                                    25.00
                                                                0.70
                                                                          0.00
                                                     25.33
                                                                ,-'-  - v,//.,,-/X;>, :„, -•. , -,,-!-- • .-
                                                                , v'""'1'"^''- ;- ;;-;•'••;-• ,j.v>!—
                                                                   •' ,,-„•< **<-.  '/'">-," , l> *
                                                                0.81      0.12
                                                     20.67
                                                     19.33

                                                     27.00
                                                               -0.80
                                                               -1.27

                                                                1.39
                                                                          -1.50
                                                                          -1.96

                                                                           0.69
0 =
     No data submitted
     Insufficient data
                              TAG SYMBOLS
                       x = Determined to be an outlier
                                                                 = Above control limit
                                                                 & Below control limit

-------
                  EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
                                                                                      14/44
Strontium-89

Lab     Res. 1
                                       Exper.   Rng anal             Normalized deviation
                   Res. 2     Res. 3     Sigma   (R + SR)    Average   (grand-avg)  (known) Tag
 RF??
 RG;;
 RJ
 RK
 RL
 RM
 RP
 RR
 RV
 RZ
 S
 sc
 SD
 SF
 SI
         22.0
          20.0
 SM
20.0
24.0
21.0
24.0
18.0

34.0
21.0
24.0
22.0
23.0
23.0

28.0
          19.0
49.0
•>;\;,-!"

22.0
20.0
20.0
20.0
21.0

30.0
 so
 SR
 ss
 ST
 SW
 sx
 sz
 T
 TPD
'•TE
 1H
 TI
 TL
 TN
 TQ
 TS
 IT
 U
 UA
 UE
 UG
         19.0
         24.0
24.0
28.0
23.0
24.0
                     23.0
                     24.0
                              26.0
15.0
42.0

24.0
17.0
29.0
                    25.0
17.0
34.0

24.0
         22.0
         27.0
19.0
29.0
                     22.0
                     29.0
 UN
 UP
 UQ
 UW
W:
                               1.53
                                        2,65
                                       s  " "" -1

                                        1.00
                                        2.31
                                        1.00
                                        2.08
                                        2.52

                                        3.06
                               4.51
                               0.58
                               1.15
                               6.51
                     1.15
                     6.56

                     0.58
                               1.73

                               1.15
                                         1.00
                                         1.00
                              0.354
                                20.33
                                                              -0.92
                                                              -1.62
                                                                     . x
                              0.236
                              0.473
                              0.236
                              0.473
                              0.591

                              0.709
                              1.120
                              0.118
                              0.236
                              2.020
                                        0.236
                                        2.020

                                        0.118
                              0.354

                              0.236
                              0.236
                              0.236
                                                    21.00
                                                    22.67
                                                    21.00
                                                    22.33
                                                    20.67

                                                    30.67
                                                    -0.69
                                                    -0.11
                                                    -0.69
                                                    -0.23
                                                    -0.80
                                                   >\0\\s-'1'':\s

                                                     2.66
                                                                         -1.39
                                                                         -0.81
                                                                         -1.39
                                                                         -0.92
                                                                         -1.50
                                                                          1.96
                                                                                        ,.*.*  •

                                                                                        ->>!-.ป'

                                                                                        0 ~\ป •
                                23.33
                                23.67
                                                               0.12
                                                               0.24
                                                              -0.58
                                                              -0.46
                                          24.67
                                          37.67  ;;ซ
                                                               0.58
                                                     -0.12
                                16.33
                                35.00
                                -vsW
                                24.33
                                                    -2.30
                                                     4.16
                                                     J.'^'.oC
                                                     0.47
                                                    21.00      -0.69

                                                    28.33       1.85
                                                                         -3.00
                                                                         ,3.46
                                                                         >r\c--ป-x
                                                                         -0.23
                                                     -1.39
                                                      1.15
                                                                                           IT
 • s No data submitted
 0 = Insufficient data
            x =
                                       TAG SYMBOLS
                                    Determined to be an outlier
                                                              ft s Above control limit
                                                              $ = Below control limit

-------
15/44 EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Strontium-89
Lab Res. 1 Res. 2
- VCJJ '••'•—'• * vf-t T? :?* $*?$
VG 20.0 18.0
vซr ,< -X';'xry^
V^^^vv^iH'!
^ VQ V -^ ''^If^tv' /E^|lf
C^4V';4;^v^5t^||i;
' v* ' ? "•" ^ ^ ';"^?"> V*'*S ^
''•**-•.. „ " •• " * ' ^ "" v >"• ;
W 20.0 20.0
X 20.0 12.0

Exper. Rng anal
Res. 3 Sigma (R + SR)
~:*"%S*,?'f ฃ*<•'' y^-'^f"™ , , . , ' '
18.0 1.15 0.236
^•:r*\''3^* •' " '' > ,\\ -
':Y-:;V ••'
l^fe^^^Kiw^'"'^ -' ''" ;'' - : '!-
^SiS^?^:^'^ ^~' ^
rMf^'^^7-:'0'^'' ' ' ,'V- ' ' '
" ^/ -"' ''"'•• ^^ ••'•• '"' J ^ "" f "y ""• '',
21.0 0.58 0.118
26.0 7.02 2.245

Normalized deviation
Average (grand-avg) (known)
' -•>. : *"• .^ vj'r.y- r;;; /'ft^^K *'
18.67 -1.50 -2.19
'''^''•'''''''v J<'''' ^ "" ' t "" "" W'f ^v' "f A * *" j'"^'^ "•"' '' """"f*
J "• "• * "s '•• ^ j ., V> "•'"' •••' "• ' * : •.\ซ.*% \f "" ., J^*'!'
, " ' '*-*'^'>:^^^~'&^^^^
•;;'>? '"^ '^-S >e?งS?iS^<^
'''^^/T-'^S^Sr^-'r!^"1
' ' •• ' ^ •• x f- -^'" *-,'•", * --^ •• >
20.33 -0.92 -1.62
19.33 -1.27 -1.96

Tag
*Vv
>^;>
vl*
$*
";ซฃ,-'
5-V
•Y.



Data sorted by Laboratory Average
Average Tag
11.00 U
14.33 U
15.00 U
16.33
17.00
18.00
18.67
19.00
19.00
19.00
19.33
19.33
19.67
19.67
20.00
20.00
20.33
20.33
20.33
20.67
20.67
20.67
21.00
21.00
21.00

• = No data submitted
0 = Insufficient data
Lab Average Tag
DG 21.00
E 21.00
JY 21.33
TI 21.33
JE 21.67
UN 22.00
VG 22.33
UP 22.33
J 22.33
EL 22.33
X 22.67
QW 22.67
K 22.67
AW 22.67
NO 23.00
HP 23.00
W 23.00
RM 23.33
BC 23.33
SI 23.33
QU 23.67
CA 23.67
U 24.00
SD 24.33
S 24.33
24.33
TAG SYMBOLS
Lab Average Tag
KX 24.67
CQ 24.67
LT 24.67
DZ 25.00
DD 25.33
BL 25.33
SF 26.00
MQ 26.33
HK 26.33
CS 26.67
SC 26.67
DO 27.00
BM 28.33
AE 28.33
NJ 28.67
DE 29.00
A 29.33
SS 29.33
M 29.67
BH 30.33
ST 30.67
1C 30.67
GQ 35.00 ft
TQ 37.67 x
JS 40.67 x
AK 47.00 x
ft s Above control
x s Determined to be an outlier II = Below control
Lab
T
DT
CJ
PB
Q
AU
CX
L
AZ
NT
AF
QZ
UE
AL
CG
C
I
BA
BO
EB
SM
FU
TL
TD
CK
RV
limit
limit

-------
                EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994          16/44
Strontium-89

 % responding labs	Frequency distribution
                    -. T.  ..filhfiiil •••  •-•_
                   r
     -6            -4           -20+2+4           +6
                    Normalized deviation of the mean from the known value


 % responding labs	Frequency distribution	
 10.	
-ฅซ-•-
                              T
                              -P
     -6            -4           -20            +2           +4           +6
                    Normalized deviation of the mean from the grand average

-------
                 EMSL-LV Performance Evaluation: Blind-B,  18-Oct-1994
                                  17/44
Strontium-90                        Statistical Summary                      193 Participants
The known value of this nuclide is 15.0 pCi/1 with an expected precision of 5.0; the control limits
are 6.3 to 23.7; the warning regions are 6.3 to 9.2 and 20.8 to 23.7
109(56.5 %) Failed to respond •
1(O.5%) Outliers	
         Statistic
                . 79(40.9 %) Within all limits
Respondents
'"•4(2.1 %) In warning zone
          but within control


             Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
     15.12
      2.93
      8.58
     19.38
      0.79
      0.04
     14.67
     -2.22
     -0.11
   Grand Avg 14.92
                2.27
                5.17
               15.24
               -0.56
               -0.04
               14.67
               -2.22
               -0.15
1(1.2 %) More than 3 norm. S.D. -.^
4(4.8 %) Between 2 and 3 norm. S.D
            .70(83.3 %) Within 1 norm. S.D.
                           of known value
      9(10.7 %) Between 1 and 2 norm. S.D.

-------
18/44
Strontium-90
Lab Res. 1
A
AE
AF
AH
AI
AJ
AK
AL
A0
AP
AH
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
cs
ex
D
DB
DD
DE
DG
DJ
pi
DM
16.0
14.0
13.0
,-' •••'- '"•"-:-
* ''"-.-.. /
17.0
15.0
15.0
18.0
15.0
14.0
16.0
12.0
16.0

15.0
15.0

14.0
•-

19.0
14.0
14.0
16.0
15.0
17.0
17.0

15.0
18.0
13.0


14.0
13.0
9.0
' -\' u
.,.,.?/; ' "v ;.ft;
* / "- ',>?•"
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Res. 2
15.0
15.0
14.0
*',7s;\?{)^
V, '• '*•'>* '•'
16.0
15.0
16.0
19.0
15.0
15.0
16.0
14.0
16.0

14.0
14.0

14.0
'' !>

19.0
15.0
15.0
17.0
15.0
15.0
12.0

16.0
17.0
15.0


14.0
14.0
6.0

: *.#. ,- ^
f;A^?-,vr
Res. 3
15.0
14.0
14.0
?-y'*/: ,-Y-//
^ 0 •,' .. i ^"" "" ' \ "h *,
' -. ^ •. \ "' -. S ., '"-•..
16.0
13.0
14.0
18.0
14.0
15.0
16.0
14.0
16.0
-
16.0
14.0
-" -
13.0
;;' '';/'' -

19.0
14.0
14.0
16.0
13.0
17.0
•• , /• ;••<•••
26.0
i' '" 1 :'-\ -,-' *
15.0
17.0
14.0


13.0
14.0
7.0
'•-" ": " \"~ '
,^ซ>T/;V/ปi
^!-<-'\-:\-;;st --'',;; ,
• = No data submitted
0 3
Insufficient
data
X s
Exper.
Sigma
0.58
0.58
0.58
!^v '; "'
"'. ' ':' - - - -;
0.58
1.15
•v "J , "* ^ <•'••,
1.00
0.58
0.58
0.58
0.00
1.15
0.00

1.00
0.58

0.58


0.00
0.58
0.58
0.58
1.15
1.15
7.09

0.58
0.58
1.00

.,,,,,,,-
0.58
0.58
1.53

'!:,;-'' '- '
^ "" ' \ % '
Rnganal
(R + SR) Average
0.118
0.118
0.118


0.118
0.236
0.236
0.118
0.118
0.118
0.000
0.236
0.000

0.236
0.118

0.118


0.000
0.118
0.118
0.118
0.236
0.236
2.245

0.118
0.118
0.236


0.118
0.118
0.354


~
15.33
14.33
13.67
>, s'! •/;'.. '..^ Kx
X^ ' ' * •• < l ,^
16.33
14.33
15.00
18.33
14.67
14.67
16.00
13.33
16.00

15.00
14.33

13.67


19.00
14.33
14.33
16.33
14.33
16.33
18.33

15.33
17.33
14.00


13.67
13.67
7.33
t f
•" ,' / , :* ' "-':
>'"' <* '•'"<.'"
TAG SYMBOLS
Determined
to be an
outlier

Normalized deviation
(grand-avg) (known) Tag
0.14
-0.20
-0.43
<; '}'-'•' '\/' ';-3l^
'">--' -, "'-- ^.H\"- ;
0.49
-0.20
0.03
1.18
-0.09
-0.09
0.38
-0.55
0.38

0.03
-0.20

-0.43
^ - "', ^ '^

1.41
-0.20
-0.20
0.49
-0.20
0.49
1.18
' •••••• -. " •••••'•• ts ;'
0.14
0.84
-0.32

. , , - , ,,,:'.
-0.43
-0.43
-2.63
.' -- , V' "'' -'s'"^ '
:jฃ't ;;/;,;„, :•'/-•„
">^'t ,. ^ ^' '*•? •• •;''%;''"•'
ft 3 Above
li 3 Below
0.12
-0.23
-0.46
^%u^V\<>i'^
*'V ;'" '"^^''^
0.46
-0.23
', " * •
'; i •' ' ' c, • -
0.00
1.15
-0.12
-0.12
0.35
-0.58
0.35
/ ' ป •
0.00
-0.23
,- ' */
-0.46
/>;V- :'\fl"
.. ; _ •
1.39
-0.23
-0.23
0.46
-0.23
0.46
~ '- ' ' *
1.15
"-•••„;•••„ /^ป"~
0.12
0.81
-0.35
. '- *
,:.:;,,,: ..= - 'ป'• -
-0.46
-0.46
-2.66
;-' 	 •'/'"
• , *
''"".'- '>' '•'.... '..*.'.
control limit
control limit

-------

EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
19/44
Strontium-90

Lab
DO

CDS-
DT
DZ
E
EB
EL

EO

EB

EV
EX

FF
FJ
FL
FN
FU
VF2

GE
GI
GQ

GT
GZ
HI
HK
HL
HP
HX
I
1C
W

'.-IB
j
JE
JG
JN
JQ
JS
JX
JY
K
: KE'
KT
KX
L
"LF:

Res. 1
13.0

>- ;^ '%>^
16.0
13.0
15.0
11.0
16.0
^ ^ -\\.. -v •v-.v •> •"• s s *


i .. •ฃ, ^ T, ^ s •• * " s1"1-.

^""•^ •••. vt\ X^sN-X V; "''
_* "- %XS-" l - ^N
> \ '>\"t ...*
0^ 0 * •. *•• tซ \ ^. ^
% i * .. v v ""' %
' '* o-s: t- ';'S
"• s * * •'^ ^ *-\ % ••
'- "f\^K>*>
	 15.0 ^
s, , ,• v-^ป x x^--™
••> ^ i •- sO' \
\ •• •• X\ o^ <" v%
>v •<
20.0


**,-** * % -.;• -
-,•."•• - *
13.0
- ••
16.0

14.0
13.0
, , - ^


15.0
18.0
x ir v
* \ V

14.0

8.0
16.0
'X ,

16.0
14.0
_•*>ซ - N, VX.^- ^

Res. 2
14.0

;"-l^'^^
15.0
14.0
16.0
12.0
15.0

";^ vx !JX*%

\\ v1"-- s - "" ^ 'X * &?
•^•^ \SC ^ ^ 1 \. ^

t'^x^N:1
.*" l:\>1'!i "%• ^ 0 % "••

:%v>V^^l;\Nx
;; -^ ^f;;;
^ '-^Jw ' "V
15.0
r/;7-:^r
\ ^% •,"" • w-
> v;>V\4:^
^ "" N s\ ^ ^
22.0

• v. "\s
'*'*•! ^^'"••"i-
- ซ_ , , "'!
13.0
'*ป'•'•
16.0

14.0
14.0
" ^ •.-. "•
, ;, -\\^ '"
" ^''^•:'^!;•\1'^--^"':: *"
15.0
18.0
^f\ " v^ t ^
' •*

15.0

6.0
20.0

."' U- - v
15.0
14.0
!f> ^, ,^

Res. 3
14.0

:,?;-> ^ '-s
14.0
15.0
16.0
11.0
16.0

,'> !- !, '-"•"

^'^'!o;V~
\i\<'\ - *f "-'- '•

;- vV-'v;\,'^
" v*'l '-\ป- ''' =

\;:.;<'J>- v-s ';
of |f;^;\'
A^f"— V: J '
13.0
^ v" "^ •• "-^ ^vX
" v \ ^ !xs

- , vV ,; ~ "
21.0


^ ' "•

14.0

15.0

13.0
13.0
.; ;,ป-s\*f " ™
•^^; \^\^ - V
"\x,""^" '• !•ซ' ' *
15.0
19.0
x > ^


15.0
-
8.0
19.0


15.0
14.0
•-> * s ^ ' •• --
• = No data submitted
0 =
Insufficient
data
x =
Exper.
Sigma
0.58

„'; , ,-\ .-^ , '
1.00
1.00
0.58
0.58
0.58

-, ' "



-- x ^ -
'x




, -\\.,-<-
1.15


' , -V ' "

1.00




0.58

0.58

0.58
0.58



0.00
0.58



0.58

1.15
2.08


0.58
0.00

Rnganal
(R + SR)
0.118

,:- - .-vO-
0.236
0.236
0.118
0.118
0.118

%> ^ \ "• % 'C^ s

, -- ,?: - ,^ _

•"-- s r=.
" v ^ ,-.'1"
"• , , "•
•• •''V,'"/



0.236


, -V-; -

0.236




0.118

0.118

0.118
0.118


,\
0.000
0.118



0.118

0.236
0.473


0.118
0.000
1 ' ,'
Normalized deviation
Average
13.67

^->''A'^
15.00
14.00
15.67
11.33
15.67

iv^*4-;t; *•;!-;

^;ซ^-i.x-' ,x

,' r^/x"V :::
\\v\\^;y^ v-;V
*• ^<-* '•Xt C1 s X ^
-f|x4$,^i;3|:
" -V-" ''•' •''„•"
-'C ! *.i~ ป ,>'
-;';*. C:^^
14.33
''"^.^X^Sf;"
••'"'•-• ^\". •. •• ^
^ --X \s tx ^ ^v^ \ -N
V - ••- •• -^-.^
21.00

>•. v - ^ ;"^ ^ ^% * \
* *\ X V
" * ^ \ ' -
, -'-V *"\V"- v'
13.33
'~'sS '-^,"%
15.67

13.67
13.33
4- ';-:-7,^<-
v^ l ^ o ^^/S' •?
"• ^ •-,_''• i.
15.00
18.33
- ^
s

14.67

7.33
18.33
^ i^ ,^;>
- -^\* ;-;
15.33
14.00
>•* *!-'" ''
TAG SYMBOLS
Determined
to be an outlier
(grand-avg) (known) Tag
-0.43

l^T^^t ^~"
0.03
-0.32
0.26
-1.24
0.26

^'\>\*"-% !~ ' ,,V/; ,ฐ0

.;1,0' --'"'';'''*' V

-CV'-;, *^!: -<•
t^f* ';!->-
^•vV ^ s 4 *"\o '"'" ^v^ "• •. s "" *•
>j->h?:;;-"f:k r"
\- ?- .\v.. ,ป- >-
i -'^X;^?": ;
^.V^\':\>0'
-0.20
^J^?7srrFv' ^
* ^ vs ^ \ % *X s v
^o vvo^x* i;J^ vi?
% ^ "*• \Tv "^ S "";
2.11

\^*v Vf"- ''*^
•.1S. .\\ v % \ %!•• s X
\%\^V " %- ^ ซ ^ ^ " ^
-0.55
- ,Vf'. i;V- ' -
0.26

-0.43
-0.55
Vx^-C^,/ ..x
\l - Xf ^N ^\^" •- ^''O1 ' ฐ--
*NV -•• "^^X --'' •xV
0.03
1.18
" - "' " ' "
f

-0.09

-2.63
1.18
"\^A? "' -" ,-
••^^ ^ ^ ^s v \~".s • s\
0.14
-0.32
V'^v'4-/- ''
It = Above
II s Below
-0.46

x'-v^'VuX" * - ^ 0s s^
0.00
-0.35
0.23
-1.27
0.23

~? ^ \" ^ , ^

' ^ ' \t, -^

- ' ' * '
, '* • -•
'
-'--vN--\v •/*,
v ••"•""" i
,:'; :--'N -•' '
;•'>>;/.;,-
-0.23
**•ฃ*•? J- * ~ •
V i^>^^ ^ __*
o^;\^-^i^ ^ ' -"• v ,
^•v>r ^ - •' •'
2.08

, 5 ," "" *
\ ' \ ' . *
;',%-;;.,/ -\vซซ, >
-0.58
'>" *:!V\~ -- •
0.23
~ซ
-0.46
-0.58
77,0' I- vป ,
"' r^"--- ^^ --v
w\w - ----''*
Of\f\
, \J\J
1.15
•
*
•
-0.12
•
-2.66
1.15
'•>r A>- ••;_;;
^ \- >' ซ"\
0.12
-0.35
' ' :T - A •• .
control limit
control limit

-------
20 / 44 EMSL-LV
Strontium-90
Lab Res. 1 Res. 2
^ jfj '"•. **** , * ••SO •-, ~ , \ ~-s ^ •" *
"• Tjfซl> >> <-'\< >' '.'oV VVov**-' *"' vV' \
: .•""""'' - .,*,,< -\- - - -; -'",,->-, ,, s ;\\
LR " •>' ^~ !- -- ^ ! r:^V"'!;:^-i--' '%•-•.',
LT 16.0 16.0
M 14.0 15.0
mjr *^ ^ "\\ / "<•.., V •. ^ t < s % "' ""*•• ฃ -^ ^ -
MA > ''ซ,•", > -A. v^;;;*',^;1
•*J*T* * ' '" •• •• V,"" 0- /Y*'\'* <•*••**
MP -> s- -'- • ,' '; -• - •<*.-. ••• 4 - --I- ซ. *•" , .,
MQ 14.0 15.0
*MV;:. ;"> -\ ' C>' VT;, J^'X;
W''-^v>;;
p • -::.^?.---i':-:
PA ^ •••';•• ^;^v
PB 15.0 15.0
PG' - , ;:,; ;, , \:^-\\
PI , \ -' ^ ": ,-- .v",
PM< r • " •, -" •'V-" ''
PQ -- ; \ r-\;-;-^
PR, ป \ • /, ,;l~
PV 12.0 21.0
'PW-- ' "" ' •'••.'," ;-'V '
Q 20.0 18.0
QC - - • -''V--> -
QJ -*^v
QP
QQ
QT
QU 12.0 15.0
QW 13.0 15.0
' CIV ' ' , -^ . -
QX-- - -, „ ,' -- -;;-,.
QZ 13.0 13.0
RCป .,,. - .... ,,.v.v,?,s ;, -,,..,
™> v V:^AV;S-^
BE"/,^ , ^ -;Jvl'"";':^C^:
• = No data submitted
0 = Insufficient data
Performance Evaluation: Blind-B, lg-Oct-1994
Exper. Rng anal Normalized deviation
Res. 3 Sigma (R + SR) Average (grand-avg) (known) Tag
,\'5- •- <;:''; *" --, -•'; -' ' " '••;'• '*-ซ,vy-^ <';:'^-^v;>yv:ปv-
N'' 'l<'" S* "* \ -i- ' %A' * ' ' ' ,.:* •• ' Av '""'"' "^ ' '"' y J/""* ^V^V^^' *.'''•• , Sr"1 S- "• "• '.
fjฎ% •>:;. •$* jl , vv ? \ s " •• ".,, •• •''•', '-' " ', ^ x , V'^ ^t^K> •• -^/ * vM^4 ft-^^'i -w^ '''"''•^ •• % '
17.0 0.58 0.118 16.33 0.49 0.46
15.0 0.58 0.118 ,14.67 -0-09 -0.12
14.0 0.58 0.118 14.33 -0.20 -0.23
: /-.. ' '•- :- -;' - ' :''"'.-'.'/'' '''" J-* ' \'- * '
; .,.-*- ' /,,-!••' , -'-,,.-,'-:, '-,'--•-',,- -• / •- ,- :•'*, ,„,- '
' v- ' ' ' '• , ' ' * ' \ •>,'',*>* ^ '*<*'> * 9,
15.0 0.58 0.118 14.67 -0.09 -0.12
,-:-•-- / - , - - -, — - , :-:~ --„-'-•:' -, ,-• -
22.0 2.52 0.591 . 19.67 1.65 1.62
16.0 1.00 0.236 15.00 0.03 0.00
' *V'?V : ,",- . •' < -'' -\\ :'; -v - -' ,'!S^i -;-/--;<,, i'ป*~ -
* - . '. .- * - - * ''•"-- /> •' ^ '" •', - \y >'",-. - *'
...: r:-\:; - •• ; • •= (- • '-'VvV./*'^-^' '-V. -7 '••"'•
;' /•,O;A''-" --' "-,-/,*- \/ ".' - '*/: - ' -, ' -•
!- :•; -- :'*-.**• r - - • , •• ,. •• -- .•..--.,• -,-sx ,,,,- ' -'
,;, -'"'•• • v ' % ' , - v •• •> -. •'•? -':-'-,•" • ~ ••"*•,,
15.0 0.00 0.000 15.00 0.03 0.00
' '' ' ' ' " ' ' s S
A % "" ^ \ V ^ / •
1 ' - ^ V ' f ' ''
* i''-" .---','' , , , - '",' -/'";"' <-: J '" - „*-
18.0 4.58 1.120 17.00 0.72 0.69
," ""'-'- - <;', ''' - " , ,' /' - y~'-X'> "';^'\--' .' •-,'
16.0 2.00 0.473 18.00 1.07 ,^1-04
_;-' , , , .*•'.'' • ' "'''•' 9 . ,
'' * '
" , _ 5 - *'','•
' - , ' , i ' ' ' 9
17.0 2.52 0.591 14.67 -0.09 -0.12
14.0 1.00 0.236 14.00 -0.32 -0.35
t , ,'
14.0 0.58 0.118 13.33 -0.55 -0.58
, s> ',,',__,.(, t '- '• '' "• ' ••,'•''•• '', - •• * V'"A ; '•!:-l!l-w ' •;V' ••••;••••'•;••'• " ^ • "
'^""'•- ••*-.,' f\ -r f •> % t ' •- , '"'"*!.'''> "" i. ""' •• ^ A'*< * ' -.-.-.' ^ /
-;f .;^;.^,>i \ ; :> •,. ;, / -'.-•-. ,•-./;/; V/-/i;r^?v ';\-v
;,r'f"i?~"""'\'"~ "" ',' ' '•' - * - , *- ' .'•' v^'v;', / "' \,\-~. *
TAG SYMBOLS ft = Above control limit
x = Determined to be an outlier li = Below control limit

-------

EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Strontium-90
Lab Res. 1
RF
RG
RJ
RK
RL
RM
HP
RR
RV
RZ
S
sc
SD
SF
SI
^'SL
SM
•^SN
SO

ii'JSR
ss
ST

SW

SZ
T
TD
TE
ATJEL "
TI
TL

TN/
TQ

TS
TY
U
UA
UE
UG

UK
UN
UP
UQ
-\UW;
-UY/
X',-Xvv tX'-S.
^ *ฐ777
- xXx%-yft
XJX^X|&|^
Res. 2
• :?:XxXX\;
X\'X'>>X7x
J^^'V^
\-v>x7'7,&
;•*'•' '- -" ,'X-
. ~J$$2 ,~
^vr^xy;X
' -X;X ~ \~X'
X^:0C!lO^^
"^'^s.|
14.0

^rfrXXX-
X~;~-v<\ --:• *
12.0
, X • '-' • ,
15.0
x1 i -

'1- s' X' - 0
14.0
16.0
~^7 ฐ:^xxn\
te&i8l5^
S;S9ISi^
Res. 3
•^,\/v ,;V
.''\ - ', > ' '
7'^xr-;
iv v X:
•>* ^ - - *
lJl7.0\


7v*8050v:
>' :-^\ V% <
15.0
15.0
17.0
14.0
13.0
__- \ __ X-v ^ •- ^ ^
13^0
•. ^ •-.*.:. -
'"•--^-.i \ : "*

S '- ~" "- ;
14.0
14.0

> - "> / • • *
\ ^r--ฐ ;-
15.0
14.0
10.0
13.0
; ^1 - ';,;-- -
17.0
15.0

^.^"•'X^X'^ ^-
15.0

s *" J s '4

13.0

15.0


\ - * "" ' .. ^
13.0
14.0
^'Jx7
(-V^i- X'~ ,,
C 'W^' :-
• = No data submitted
0 s
Insufficient
data
X =
21/44
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
,,-

- 1 „ - =


1.00
J *^ , ^

7 5.29^--
1 ;-
0.58
0.00
1.00
0.00
0.58
,~ -, ,'''",-
0.58
-"' "•" 7,' "-'X
-- - \': ^\ "

""" siX •• ;•'•-.
0.58
0.58



0.58
1.15
1.00
0.58

1.15
1.15

X ~ . "•' *'*'** "
1.00



0.58

0.00



0.58
2.00
- V\'/ ~c

~'" \' X • !\ -"
' - !

5 _, - ^ s


0.236


1:348

0.118
0.000
0.236
0.000
0.118

0.118
s ^ •"'SA.
/ ' - X


0.118
0.118



0.118
0.236
0.236
0.118

0.236
0.236


0.236



0.118

0.000



0.118
0.473


* -. ' ' ^
XX "Xr J^V ;x-
;'7^>" N' v'^xV'
'>;'-> '-'\4>">\\

; . ' ' x *- • x-' .! . ซ -
16.00
v , s ^ ^ -.
\ - N \ " "
;7"~:7 32;OQ>^t-
X ^^ -S " S"J - s \^V -\
14.33
15.00
16.00
14.00
13.33
ฐ* - X.XX X:? X
1 	 12.33_
' - J \ ^ ^ " -.™\v.^ ™\^s _*
\ ; K * x -."•••-x

7 7'' ''7'- '^57^
14.33
14.67

~- - , - -^v i o
, ' ' -- x ^X' Ivv
14.33
12.67
11.00
13.33
-•••• i %< "• % " -•X'- " ^-^s*
17.67
14.33

, , . ' ,"' ,;," };! *5
14.00

'• \ ' - , ,\ '-\T ,:;
' 7- ^ :
12.67
> •" v -
15.00
^^ - o sซ. "" -

" ' • - - X>,' ' ,
13.33
14.00
\ r\x, X'-'v^
777-, •' 7;X,vtj'
, '•*'* X \>^ -^^^-'i
TAG SYMBOLS
Determined
to be an
outlier
7>^:^C:7VS^
f^'c-Hv^v-)^
:xv;b;S7^^
^TCvx^^^
V*1 ''*••'•'' \ s*o ' N -
^ x x •• \ •. s
J_0.38
ป-,,-;xx ; -a •/„„.
-,': , ;';\f'- - '7
";;&9%X-"
*_^'" "\-,-l -1-'
-0.20
0.03
0.38
-0.32
-0.55
XXx"-::
-0.89
T^{X"X;rX':;
' y"!-xj •> V;>" 5 ,;' ^v1* ^

, >-,>v "!~-,\^x->~^ \^
-0.20
-0.09

,' N*,V\~** \ ฐ '^
'"X-iVrX^'77--
-0.20
-0.78
-1.36
-0.55
- ^'-.7 \\^\o % , ••'V''
0.95
-0.20

IvX/vS ' ;3' X
-0.32

_%ซ. •. •.ซ ^^ •• s
y \ - x" <\
-0.78
:"??'\-:i' ,
0.03
'^XX"' -;i;-'^
- % •• -

-0.55
-0.32
--\- ^ A "• "• .jj, v t ;'*• \
"7i! I XX; ;XX'
s,^ v *xv ;-. -* ^ - ^ ^s- v--
.<:^~^ v\<"v;;v, '- , ,
IT 3 Above
U = Below
^XXX:;X ซv'.
|>?:X;77^ป7^
xT&vS-X
\\ ""*% *"* ^ t1"" N S\ "*
%v ^ •, % '"'•'•- ^
0.35
7 7- '; ' •"' '
. ,;1- \ - •
^89 % ^x
- - , *
-0.23
0.00
0.35
-0.35
-0.58
'XXX xXซ-
-0.92
\"ST\'Xi"ป\r
5- *•*• Af "•ji-.t A 5 v '-.
4s**- v- ^ '^"^X-x \ * *\ •>

>5t^'-sX •"<>-'
-0.23
-0.12

• , - • ', N • •
- ^ ,* % ..- ^ '
-0.23
-0.81
-1.39
-0.58
XvXX5 >vซ " "
0.92
-0.23

X-X5XX\ *VA
-0.35

T ;,-:;'- -- > ^ _
ซ
-0.81
> - • ~ - ซ ,
0.00
\ { -,.- ; ^ .

<,. t *; : ~; ซ
-0.58
-0.35
;f?ปฃxV',:''"ป
"r,7^,S! vป-r
^Cv"X>^ป <
control limit
control limit

-------
22/44 EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994 1
Strontiiun-90

Lab Res. 1 Res. 2
- vo A :-v\ " >^ ^ ^r-,^^^r^
VG 17.0 18.0
•• , v , -.-•-' , -r '-z\ ',.*'> •"•e^v <•-
VJ \ .^ - y -f^ ~; V",
"Vซf~'' '' — '- *"•'<•' * s^-'^K-i&
-' A*ปo% "V' •ป'ป'> ซ%vY's *r>'s, ?V--

"VN:^:;^';^,;^;^-;l::^
VO 23.0 23.0
__ t. •. J •• ,". •• :
'" VQ*: \ - , ?", '- ^-" ^ ^:-
"%/lT* " ' ..*?"• \ts ' ."••% X*;- ••
T •.ป •> *• , "• % N > •• v' ' i % 4 '*•"•"•
VU:-; \;fX-'^:4<
-"VX- ' ' ' - - ' - "--'"'- - -
' -.^ •. ''-,'•••
W 14.0 15.0
X 15.0 18.0

Exper. Rng anal
Res. 3 Sigma (R + SR)
^;;t3\;^ V;-. -;;'.' , :; :' .
17.0 0.58 0.118
\ฃ& ' ''''--"'iT^V'F!;'^' •"" ;* ' - '
,,,-i<;;>:f- ./;, CrJ\ „- /- - • -;
\^-::v>'<^;>- :„-•!:, /T, - -1 ," : - -
" f < ซ> • f , >- , f -;v, S - ; ,

\;^''^,y^:<^ : '!\f A-\
21.0 1.15 0.236
•' ^' '•S 'f :•• f
•3 "\ *y,: *i- 'V,1"' * " •" *• ' -'
'•"-\:> '>.',!V\^r -' '>
;-\<;-V.<--/' ' :^ ;•,/-' ,'-/
* - t "" -. ..' ^ ^ '
v "" 'i- "• •. ^ -.
15.0 0.58 0.118
14.0 2.08 0.473

Normalized deviation
Average (grand-avg) (known)
•'• ,:--";vy; /'-'„;> ,"Xv'^--T.' >"
17.33 0.84 0.81


Tag
; .'#-, ;

".Y"" "*".. \'?'"'"Y">?^::^\^ซ^
' > y :':'-'- \-(>"> ''^-^ ^": ^$>"$! \-ฃ&. i&
J -."•'"'• ^ s s ^ v*^ s 4S'- ••''* ', * '^ ' -'--- '->;"-'- -^^-^'C'^''0''1""" '"i-*1"-;0 ''''
'•"<•{>'• -'='>' v^^^"-!., r-> ^'^!4^-/' "'.'I*-
22.33 2.57 2.54
•- sfc A^^%\^
", '" '\ , _ *'"'"* '*~^'*'\' "'• "?<'„->,- ซX';"_~";';-™"^-'
'- - -;/' ''- S'^' ' '"'; '-'""' '.i'v*^'
-;-/ ;,-; Nv --Y' ;,--,"•'"*' --f^r"
- •-..",;, - "- '-, -;'",.,'''* V v^;- " ' .-,--
^ '.-'*,' -'
'*''.'' ' * * * * *-..-*'"' %%r^
14.67 -0.09 -0.12
15.67 . 0.26 0.23
•;>', '
v •V
t \ •. '
•"""•^A ^\ /
>v^


'-=*,! '
, •*- '
!.;X '' 5
•



Data sorted by Laboratory Average
Average Tag
7.33
7.33
11.00
11.33
12.33
12.67
12.67
13.33
13.33
13.33
13.33
13.33
13.33
13.33
13.67
13.67
13.67
13.67
13.67
13.67
14.00
14.00
14.00
14.00
14.00
14.00
14.00
14.33
• = No data submitted
0 = Insufficient data
Lab Average Tag
JY 14.33
DG 14.33
TD 14.33
EB 14.33
SM 14.33
U 14.33
T 14.33
UN 14.33
TE 14.33
SI 14.33
QZ 14.33
1C 14.67
HK 14.67
BG 14.67
I 14.67
DO 14.67
DE 14.67
DD 14.67
BO 14.67
AF 15.00
UP 15.00
TQ 15.00
SF 15.00
QW 15.00
L 15.00
DZ 15.00
CX 15.00
TL 15.33
TAG SYMBOLS
Lab Average Tag
SZ 15.33
SS 15.33
S 15.67
MQ 15.67
FU 15.67
CJ 15.67
CE 16.00
CA 16.00
BM 16.00
AL 16.00
AE 16.33
W 16.33
ST 16.33
QU 16.33
NJ 17.00
M 17.33
JS 17.33
BA 17.67
AZ 18.00
UE 18.33
SC 18.33
PB 18.33
NT 18.33
J 19.00
DT 19.67
BL 21.00
AU 22.33
KX 32.00 x
IT = Above control
x = Determined to be an outlier & s Below control
Lab
CQ
A
X
HP
EL
E
SD
RM
BH
BC
LT
CK
CG
AK
PV
VG
CS
TI
Q
K
JE
CO
AW
C
NO
GQ
VO
RV
limit
limit

-------
                EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
                                                                                  23/44
Strontium-90

 % responding labs

 20

 10

  o-L
     •6
                                 Frequency distribution


1
II
1
1 	
1


...L. . .




B
                 -4            -20+2+4
                    Normalized deviation of the mean from the known value
% responding labs
204	
                                  Frequency distribution
 10-
     -6
                 -4            -20            +2            +4
                    Normalized deviation of the mean from the grand average

-------
                 EMSL-LV Performance Evaluation: Blind-B,  18-Oct-1994
                                  24/44
Cobalt-60                           Statistical Summary                      193 Participants
The known value of this nuclide is 40.0 pCi/1 with an expected precision of 5.0; the control limits
are 31.3 to 48.7; the warning regions are 31.3 to 34.2 and 45.8 to 48.7
67(34.7 %) Failed to respond
8(4.1 %) Outliers •'
         Statistic
                111 (57.5 %) Within all limits
Respondents
—— 7(3.6 %) In warning zone
            but within control


               Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
     40.54
      6.49
     42.09
     16.00
      1.36
      0.08
     39.33
     -1.67
     -0.10
     Grand Avg  39.43
                  2.65
                  7.00
                  6.71
                 -1.43
                 -0.22
                 39.33
                 -1.67
                 -0.25
8(6.3 %) More than 3 norm. S.D. ป„
7(5.6 %) Between 2 and 3 norm. S.D.
             86(68.3 %) Within 1 norm. S.D.
                           of known value
    * 25(19.8 %) Between 1 and 2 norm. S.D.

-------
25/44
Cobalt-60
Lab Res. 1
A
AE
AF
AH
AI
AJ
AK
AL
AO
AP
AH
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
BS
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
CS
CX
"i>
DB
DD
DE
DG
IDJT
DL
DM
• =
0 =
32.0
35.0
41.0
>• V^x.;*
40.0
ป, ' ,i, ' - 1 .. <. -'
38.0
'• - 4%X)
••.v>\v-",:>y.
37.0
'*-.'• '- •.'""•.
41.0
35.0
30.0
41.0
38.0
39.0
39.0
40.0
41.0
39.0
36.0
• ' '' , -, ;: '' '
53,0?
38.0
40.0
40.0

40.0
43.0
45.0
41.0
40.0
43.0
43.0
43.0
86.6

32.0
40.0
41.0
36.0
42.0
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Res. 2
32.0
35.0
39.0
*-", , ^-ff,\ >"'?*-'-,
41.0
„'• ^sJ-Ho^-
37.0
''"•', 66.0 ^
>,/,^yซ'/\y.
44.0
39.0
35.0
41.0
39.0
38.0
39.0
39.0
37.0
39.0
39.0
42.0
-s, -Y , ,",•
-•; :46.0
40.0
43.0
41.0

41.0
42.0
44.0
37.0
40.0
47.0
44.0
45.0
71.0

35.0
40.0
40.0
38.0
40.0
Res. 3
36.0
39.0
37.0
^:H^'hvi
41.0
^v/-\ -.^ j.
39.0
<^"49ป0'-''
,Y'V'~S/'
35.0
v w .?"*• \ __ ซ-, •• ,
39.0
40.0
34.0
41.0
39.0
*/-'6LO-'-
40.0
38.0
39.0
43.0
39.0
37.0
•/ .?.,\
-: S3.0,
40.0
39.0
40.0

42.0
42.0
49.0
39.0
41.0
48.0
45.0
52.0
76.0
x - ' <
32.0
40.0
40.0
c ^- ^ -* ^ /• - ^^
40.0
42.0
No data submitted
Insufficient
data
x =
Exper.
Sigma
2.31
2.31
2.00
c^V ^\{ - -"';• -
0.58

1.00
V/^ 4.36
~"; --.-'-,-' -:* ••
• 4.73
1.15
2.89
5.57
1.15
0.58
0.58
0.58
1.53
2.00
0.00
3.21

V 4:04
1.15
2.08
0.58

1.00
0.58
2.65
2.00
0.58
2.65
1.00
4.73
; 7.64

1.73
0.00
0.58
2.00
1.15
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
0.473
0.473
0.473
/- :':
0.118

0.236
; 0.946
* *'
1.120
0.236
0.591
1.570
0.236
0.118
0.118
0.118
0.354
0.473
0.000
0.709

0.827
0.236
0.473
0.118

0.236
0.118
0.591
0.473
0.118
0.591
0.236
1.120
2.470

0.354
0.000
0.118
0.473
0.236
33.33
36.33
39.00
S / ' ''- ' V-V-i'"^
40.67
- '- <- - :ซ--v -
38.00
'- 51*00; \-
", /-' " " ' -;i"r-
38.67
39.67
36.67
35.00
40.33
. 38.33
39.33
38.67
38.67
41.00
39.00
38.33
" •••
50,67
39.33
40.67
40.33

41.00
42.33
46.00
39.00
40.33
46.00
44.00
46.67
77.67
' ' '
33.00
40.00
40.33
38.00
41.33
TAG SYMBOLS
Determined
to be an
outlier
-2.11
-1.07
-0.15
^f^l^.f!%-
0.43
^.•VY^V-.';
-0.49
s\!40i!'r^~':
•;/;' '"" ;}•,<.""•ป••••''
-0.26
0.08
-0.96
-1.53
0.31
-0.38
-0.03
-0.26
-0.26
0.55
-0.15
-0.38
"• , - - ,-, ;,:-
3;89
-0.03
0.43
0.31

0.55
1.01
2.28
-0.15
0.31
2.28
1.58
2.51
13.25

-2.23
0.20
0.31

-0.49
0.66
ft s Above
•li = Below
-2.31
-1.27
-0.35
\v 1 ™ ฃ^fj&.
0.23
*^>':--'ป*f
-0.69
3^81 x
/ ' '/-"-' ,'*-""
-0.46
-0.12
-1.15
-1.73
0.12
-0.58
;:-r?^ "0-
-0.23
-0.46
-0.46
0.35
-0.35
-0.58
- -,7 'V • /
3 JO x
-0.23
0.23
0.12
- - • -;
0.35
0.81
2.08
-0.35
0.12
2.08
1.39
2.31
13.05 x
.ป '
-2.42
0.00
0.12
•
-0.69
0.46
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cobalt-60
Lab Res. 1
DO
BS
DT
DZ
E
EB
EL
JKp7
ER
-EV-
EX
FF
FJ
FL
:FN
FU
FZ
GE
GI
GQ
GT
GZ
HE
HK
HL
HP
<* HOC ,
i
1C
m
nee.
j
JE
JG
JN
JQ
JS
JX
JY
K
KE
KT
KX
L
LF
• =
U-
39.0
41.0
35.0
40.0
39.0
42.0
'"•,'* s ^v\ '•' ' "" ^ v* '"'
42.0
38.0
39.0
,
40.0
43.0
40.0
38.0
41.0
- ."i-A *
40.0
41.0
37.0
\ ซ: ,
43.0
40.0
- ^ % "" \ %
39.0
38.0
39.0
- X
38.0

45.0
35.0
X "
,.
40.0
38.0
37.0
Res. 2
39.0
4LO
36.0
40.0
39.0
<~-4^k^
Sf-'^sp^* v!
39.0
39.0
41.0
•-
40.0
45.0
38.0
41.0
41.0
's-X - ^~ ''•!'-"'
40.0
41.0
40.0
< \
42.0
41.0
- •> •ป ••'<• ^ " s t ^ฐฐ
40.0
40.0
41.0
^
36.0

47.0
33.0
x V
1< % -v
38.0
38.0
38.0
Res. 3
35.0
39.0
35.0
41.0
39.0
39.0
" '^I*1^
41.0
40.0
41.0

41.0
46.0
36.0
39.0
43.0
^ 1 - N J
* "• •? "
vป , <'"s -
40.0
41.0
39.0
*
39.0
41,0
^Fc"<
39.0
39.0
38.0

37.0

42.0
34.0
s
\
36.0
42.0
37.0
No data submitted
Insufficient data x =
Exper.
Sigma
2.31
1.15
0.58
0.58
0.00
1.73
V.-- v' " '
1.53
1.00
1.15

0.58
1.53
2.00 .
1.53
1.15
'~
0.00
0.00
1.53

2.08
0.58
^
0.58
1.00
1.53

1.00

2.52
1.00


2.00
2.31
0.58
Rnganal
(R + SR) Average
0.473
0.236
0.118
0.118
0.000
0.354

0.354

0.236
0.236

0.118
0.354
0.473
0.354
0.236

0.000
0.000
0.354

0.473
0.118

0.118
0.236
0.354

0.236

0.591
0.236

"
0.473
0.473
0.118
TAG SYMBOLS
Determined to be an
37.67
40"33
35.33
40.33
39.00
40.00
x', - . ' ซ
40.67
- ol '--=, \-X~
39.00
40.33
*
40.33
44.67
38.00
39.33
_ 41.67^
, * - : ", " " •• -x -
40.00
41.00
38.67

41.33
40.67
- ^•>>'--'"-\!'-x
39.33
39.00
39.33

37.00

44.67
34.00
, . '-v>\

38.00
39.33
37.33
outlier
26/44 I
Normalized deviation
(grand-avg) (known) Tag
!1^'":>^
0.31
-1.42
0.31
-0.15
	 0.20_^ _
A!X'X:-\ ';,: -'-'
0.43
-0.15
0.31
v A x
0.31
1.82
-0.49
-0.03
	 0.78_ v%
:-%-vA-s ^^"" -;
0.20
0.55
-0.26
\
0.66
	 OA3 	
s % C" •.' s
-0.03
-0.15
-0.03
s *^"
-0.84
<
1.82
-1.88
; v "
v" , ^ -
-0.49
-0.03
-0.73
ft 3 Above
li s Below
-0.81
0.12
-1.62
0.12
-0.35
0.00
\ '~; \ .* ' - -
< ^V" --ซ- -
0.23
- , '*,-!,'••>
-0.35
0.12
.^
0.12
1.62
-0.69
-0.23
^0.58
^xv^\^^ > * ^ •
' ' '.x- "'*
-'- ; ' \*
0.00
0.35
-0.46
•
0.46
0.23
-V"*:V,,^*
-0.23
-0.35
-0.23
^
*
-1.04
•
1.62
-2.08
1 •
^ " *
-0.69
-0.23
-0.92
control limit
control limit

-------
27/44
Cobalt-60
Lab Res. 1
v "• v ., v*x
";LLc
LR
LT
M
MA
MP
MQ
MV
MY

N

-NA
NH
NJ
NK
NO
NT
O
OF
OS
-' tyv

OY
P
PA
PB
PG
PI
PM
PQ
PR
PV
PW
Q
QC
QJ
QP
QQ
QT
QU
QW
QX
QZ
RD
,
RE)
• =
0 a
JV';^1t>
->?';,<• ^V-'^A,'
41.0
38.0
38.0
43.0
35.0
38.0
36.0
' 73.0



j \S s •. •- ^ v ^
41.0
38.0
41.0
""/ ' 23.0} ';

41.0

' '•• -.-." -" - '- .
..; f ^


55,0;

40.0

38.0
46.0

- ' ;, -'-
42.0
37.0
39.0

40.0
38.0

37.0

'
49.0
37.0
* *' ' **"•'*' * '

X' ', \ V.. <** \
^
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Res. 2
jS;|fO
)|/V> >^;fV'-
36.0
40.0
38.0
41.0
36.0
38.0
39.0
74.0



-•••. {,V
37.0
38.0
40.0
;'^2e.&
:''• '•*' SP
41.0
'' vv^:
,- -! * ' V '' *' V,
t -. ^ ''

\ ' ;,''-
66.p

39.0

38.0
44.0


41.0
35.0
38.0
" * •• , "' s" *
44.0
37.0

38.0


50.0
36.0
'.-' - ,':-
^ '' "• *. "
' ' "" -*•.';' ^ ^
Res. 3
*S:?1S
;3ff>>fe^€:t.>,^
44.0
36.0
37.0
41.0
35.0
39.0
37.0
''• '?v'73.6'"
.. A ' ,


-V- ',-.'-> "^ '^-VX"
37.0
39.0
40.0
J;>; V?&Qf
f--?', ;•'*' - ,
42.0
~\\\-^:^\'i
••'•ivVv .'-'/•
s Atj ,;4, \/ , '•

';•.-. \ 2152, _
:~ , ' ,
0.58




^ \ '' ' ~- -.
\ '
2.08

0.58

0.58
4.73

"
2.65
1.00
1.00
s1" '"''
2.65
1.00

0.58
•. f

0,58
0.58

' '" , " '
.;,^-'-~ - -V - .ซ••'-•
Rng anal
(R + SR) Average

:'-~,,:W
0.945
0.473
0.118
0.236
0.118
0.118
0.354
0.118




0.473
0.118
0.118
0.591

0.118





0.473

0.118

0.118
1.120


0.591
0.236
0.236

0.591
0.236

0.118
.,

0.118
0.118


•• .-.•-• - , .; , ,
,;*': 'V'/:S>;
*••*•• ^'A~ Ji;^-i
40.33
38.00
37.67
41.67
35.33
38.33
37.33
" " ..: 70133 ;ป'
, s>


- •", -->.:!/ \-
38.33
38.33
40.33
" '."" 25;67V

41.33
' ' ""'•" r J
' ^ , " * ' ^ '" ''' ' \



;5433

39.67

38.33
42.33
•• 0 , ^ l
'""'•-, ^-' ^
43.00
36.00
38.00

41.00
37.00

37.67
' "

49.33
36.67
- / ' " " : , '''

, -:i ' " \f ,''• : , s!, „'
TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known) Tag
^l'K;K7S
^^^^C'.^c-;'
0.31
-0.49
-0.61
0.78
-1.42
-0.38
-0.73
•' •, 11.76 v,V •'•,---

, • i _ ';

- ' " " -. >'', ,V ,',
-0.38
-0.38
0.31
v' ' * *1-*'; **•" , s

0.66
V:<-'' •:'-ป"'' \/'
s r* ^' " •• ^ ^
v- ^^ v

'' *. %'V1 -. f ',-••.' "•
5,16
V * " s'
0.08
-•-'•• •" '•' ' '
-0.38
1.01
•- ' • < '
* * "' , '~.~"-
1.24
-1.19
_ :0.49 	
-* ' '"'.""
0.55
-0.84

-0.61
., ,,.. ,; ..;,,,,_

3:43
-0.96
•'' '-"''• '-;--:; I.':'1
•^ ; -.- " ' ">
- ~- ' >.-l '-vซ ; ;'.
tt = Above
Ji s Below
/- '1't-;'''?i<^- *V
"^; j;,|S t* ^y*-;**-
0.12
-0.69
-0.81
0.58
-1.62
-0.58
-0.92
iL55"- ' - '• xx" -

• ; -

< O/.V''^'*".."'
-0.58
-0.58
0.12
,.4.,9;7- ',•;*;:'
0. \-" ^ซ -
0.46
;ฃ :-'f ! v -(!
PV: •ป'".' 1- Vf ; V
i -\ '-#' ••

r'V""--''.*'"
' 4 ^^ ' - x
.' ' :- , : • ->.* -'--
-0.12
-/'' <'':'-V\;
-0.58
0.81
1 : ' //* •'
'-^'/V-' ,rซ .'.-',
1.04
-1.39
-0.69
; - ^ , ;;-* _ -'
0.35
-1.04
-•.-
-0.81
'' ,-, ' , - \*,
" ;ป ,
3.23 k
-1.15
->;';:•;•/•:• ••

^V^',', ,"s ,;„•'*;ซ',..
control limit
control limit

-------

EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cobalt-60
Lab Res. 1
RG
RJ
RK
RL
RM
RP
RR
RV
RZ
S
sc
SD
SF
SI
''SL>
SM
SN
SO
SR
ss
ST
SW
sx
sz
T
TD
TE
TH
TI
TL
TN
TQ
TS
TY
U
UA
UE
UG
UK
UN
UP
UQ
UW
UY
;- vr?S
- • :• '•
37.0
39.0
39.0
33.0
42.0
41.0
45.0
35.0
38.0
'-, : \ - -">'*• o
33.0
40.0
38.0
" *-A "-"^ •• "*"•;•
40.0
40.0
38.0
41.0
39.0
43.0
42.0
38.0
\ ""
38.0
34.0
41.0
39.0

50.0
41.0
36.0
41.0
46.0
Res. 2
,\;ff 4" ••"' ,,r
'' \'\\b^''"-<*
39.0
s ^ \ 5 !v -. ^ %
38.0
40.0
34.0
39.0
45.0
37.0
4
35.0
39.0
. :.;;:'; n\ 'c-
36.0
41.0
	 ^ 37.0 ^
39.0
41.0
37.0
40.0
39.0
45.0
42.0
37.0
^ "\C" ป
37.0
35.0
41.0
41.0

47.0
41.0
37.0
44.0
41.0
Res. 3
":, ,>% \\.
%'. •> -.'-X ;<-
* 36.0
40.0
40.0
36.0
41.0
39.0
42.0
36.0
38.0

41.0
40.0
35.0
39.0
39.0
37.0
40.0
40.0
43.0
45.0
35.0
X
38.0
37.0
41.0
40.0

48.0
42.0
38.0
44.0
42.0
• = No data submitted
0 s
Insufficient
data
x =
Exper. Rng anal
Sigma (R + SR) Average
,- * • - '' : '
,,-.ซ> -
1.53
\, ' :4.51 .'
1.00
0.58
1.53
1.53
3.06
4.04
0.58
0.58 .

4.04
0.58
1.53
0.58
1.00
0.58
0.58
0.58
1.15
1.73
1.53
.
0.58
1.53
0.00
1.00

1.53
0.58
1.00
1.73
2.65
r*--\ :
.-7V,"1"
0.354
* s
L12Q
0.236
0.118
0.354
0.354
0.709
0.945
0.118
0.118

0.945
0.118
0.354
0.118
0.236
0.118
0.118
0.118
0.236
0.354
0.354
•"•
0.118
0.354
0.000
0.236

0.354
0.118
0.236
0.354
0.591
V^^-v
v. !;; c|r>
37.33
'•V !l" 74/33"
39.00
39.67
34.33
40.67
41.67
41.33
35.33
38.33

36.67
40.33
36.67
39.33
40.00
37.33
40.33
39.33
43.67
43.00
36.67
%
37.67
35.33
41.00
40.00
X-\f -'
48.33
41.33
37.00
43.00
43.00
TAG SYMBOLS
Determined
to be an
outlier
28/44 |
Normalized deviation
(grand-avg) (known) Tag
;^J-5^^ง:X
- •; V^ . J V" - '- -
'•f:^i^:r^
-0.15
0.08
-1.76
0.43
0.78
0.66
-
-1.42
-0.38
J' •*~>l- sป ,;S;X^ ป>
-0.96
0.31
-0.96
-0.03
0.20
-0.73
0.31
-0.03
1.47
1.24
-0.96
-\ , " V
-0.61
-1.42
0.55
0.20
y";1' ->' „
3.09
0.66
-0.84
1.24
1.24
It = Above
U = Below
|vv;-;ซ;;
%lis^ *'"ป••ซ;.
-0.92
11.89 x
-0.35
-0.12
-1.96
0.23
0.58
0.46
*
-1.62
-0.58
"" \V ^5^ v •• ^ s ^ v •> Q \
-1.15
0.12
-1.15
-0.23
0.00
-0.92
0.12
-0.23
1.27
1.04
-1.15
V •
-0.81
-1.62
'• *
0.35
0.00
v\'- '•
2.89
0.46
-1.04
*
1.04
1.04
control limit
control limit

-------
29/44 EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cobalt-60
Lab Res. 1 Res. 2
VC 43.0 43.0
VG 39.0 42.0
_.__-. %s __ •• "... ;'v ••' \
"VI*^ / """ - C!X-V : "" "i "" "- < '- ^ v'V "
'>J\\; -'/:,v-i:ซC
VN :O- - vฃ ;;''' .,'*- -v-
VO 41.0 41.0
VT 30.0 37.0
VU 38.0 37.0
vx .-• • \-.'-\ :•, v- M
W 38.0 39.0
X 38.0 37.0

Exper. Rng anal
Res. 3 Sigma (R + SR)
39.0 2.31 0.473
35.0 3.51 0.827
""' '' s "1'^ i '""V* ' % "• s "s *• *% ' '
' ^ ' *5" '' ""f •• ^ \^ -"" "" "" ' " S , ^ "" ' ^ ""
:'":" -v\ ''-?\-* " ' • / / -- '
-1 s s ^'••^. ., , -.^ 0 v A\-- / , \ "" -.--•-
,49;9 ฐ;58 ฐ-118
43.0 6.51 2.020
38.0 0.58 0.118
' '-\,V'Kx; -N -* -'-' -:-.-'•
35.0 2.08 0.473
44.0 3.79 0.827

Normalized deviation
Average (grand-avg) (known)
41.67 0.78 0.58
38.67 -0.26 -0.46
%* s < .. ' ••**••' •• ^ .. .. ^ --V *^y.ซ * t „ •.
• ' "• -: 'vv*?-'' '- " ' "*'•' JvHx A*fiฃซ*
- * > •- , '* •• ' ? s 'j o r" **-,<• •• ? ' ,-/^ ,,'f •• ''
''' , •*''',-. *\** '•• ..•-''* ~s '']-.^\'-J 'Vs-^v'x
-,,--- -s, •'•"',"* ,',X"' ''-',,V^X ,^ ,"
40.67 0.43 ,,,0:23
36.67 -0.96 -1.15
37.67 -0.61 -0.81
- ' ''>. / X '•?';',*;;„ - iv'">',- -^-'U"'' *' *'
37.33 -0.73 -0.92
39.67 0.08 -0.12


Tag



T"' i*j,:5-
l$;l
:^:
V , , , *


' •*•/ :


Data sorted by Laboratory Average
Average Tag
25.67 x
33.00
33.33
34.00
34.33
35.00
35.33
35.33
35.33
35.33
36.00
36.33
36.67 '
36.67
36.67
36.67
36.67
36.67
37.00
37.00
37.00
37.33
37.33
37.33
37.33
37.33
37.67
37.67
37.67
• = No data submitted
0 = Insufficient data
Lab Average Tag
NO 37.67
DD 37.67
A 38.00
K 38.00
SC 38.00
AZ 38.00
TS 38.00
SM 38.00
MP 38.33
DZ 38.33
PW 38.33
AE 38.33
VT 38.33
TL 38.33
ST 38.33
SR 38.67
QZ 38.67
AW 38.67
UP 38.67
QP 38.67
JS 39.00
W 39.00
T 39.00
RM 39.00
MV 39.00
LF 39.00
VU 39.00
TQ 39.33
QT 39.33
TAG SYMBOLS
Lab Average Tag
M 39.33
DO 39.33
Q 39.33
LT 39.33
KX 39.33
GE 39.33
DL 39.67
AK 39.67
SN 39.67
PI 39.67
NJ 40.00
NH 40.00
MQ 40.00
BO 40.00
BC 40.00
VG 40.33
HP 40.33
BL 40.33
BK 40.33
AP 40.33
RZ 40.33
JE 40.33
FJ 40.33
EB 40.33
CO 40.33
BN 40.33
AF 40.33
TE 40.67
SX 40.67
ft = Above control
x = Determined to be an outlier li = Below control
Lab
L
JG
J
GI
C
BH
X
S
PB
AU
UE
SZ
HK
EL
DE
TD
SS
NK
LR
FU
FL
E
DT
DG
CP
CE
BA
VO
SD
limit
limit

-------
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cobalt-60

30/44

Data sorted by Laboratory Average
Average Tag Lab
40.67 1C
40.67 EX
40.67 CA
40.67 AI
41.00 U
41.00 QJ
41.00 HL
41.00 CJ
41.00 BM
41.33 UN
41.33 SI
41.33 O
41.33 I
% responding labs
Average Tag Lab Average Tag
41.33 DM 44.67
41.67 VC 44.67
41.67 SF 46.00
41.67 MA 46.00
41.67 GQ 46.67
42.33 PM 48.33
42.33 CK 49.33 x
43.00 UY 50.67 x
43.00 UW 51.00 x
43.00 H 54.33 x
43.00 PV 73.33 x
43.67 TH 74.33 x
44.00 CS 77.67 x
Frequency distribution
Lab
JY
FZ
CQ
CM
CX
UK
QX
BW
AL
P
MY
RV
D



IU' -----------------


-A -4
	 	 • 	 	
Bi|HU
. .-•-llllltllll.l 	 . 	

-2 0 +2 +4


m

+6
Normalized deviation of the mean from the known value
% responding labs

|g. _-_______-_------


-6 -4
Frequency distribution

;:::::::::;;;;;;:::
•-•__. . 	

-2 0 +2 +4



_ m

+6
Normalized deviation of the mean from the grand average
• = No data submitted
0 s Insufficient data
TAG SYMBOLS ft = Above
x = Determined to be an outlier •!! = Below
control limit
control limit

-------
                 EMSL-LV Performance Evaluation: Blind-B,  18-Oct-1994
                                  31/44
Cesium-134                         Statistical Summary                      193 Participants
The known value of this nuclide is 20.0 pCi/1 with an expected precision of 5.0; the control limits
are 11.3 to 28.7; the warning regions are 11.3 to 14.2 and 25.8 to 28.7
67(34.7 %) Failed to respond
5(2.6 %) Outliers -'
         Statistic
               . 120(62.2 %) Within all limits
Respondents
1 (0.5 %) In warning zone
       but within control


          Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
     19.16
      4.05
     16.38
     21.12
     -4.18
     -0.21
     18.33
     -8.33
     -0.41
Grand Avg 18.45
             1.78
             3.16
             9.64
            -7.73
            -0.87
            18.33
            -8.33
            -0.94
5(4.0 %) More than 3 norm. S.D. .„
1(O.8 %) Between 2 and 3 norm. S.D.'
             89(70.6 %) Within 1 norm. S.D.
                           of known value
     31(24.6 %) Between 1 and 2 norm. S.D.

-------
32/44
EMSL-LV Performance Evaluation: Blind-B, lg-Oct-1994
Cesium-134

Lab
A
AE
AF
-ABtc
AI
AJ:
AK
AL
V Arf"^''%
,--Av
AP
AR
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
B8
BW
C
CA
CE
CG
CJ
CK
CM
CO
CP
CQ
cs
ex
D
DB
DD
DE
DG
DJ
DL
DM
• =
0 3

Res. 1
15.0
17.0
16.0

18.0
, v
20.0
18.0


20.0
-•' > / • _,.
20.0
19.0
19.0
17.0
17.0
23,0
16.0
18.0
20.0
19.0
17.0
18.0

37.0
17.0
20.0
18.0

20.0
20.0
21.0
20.0
18.0
20.0
20.0
23.0
39.0

16.0
19.0
18.0

18.0
21.0

Res. 2
15.0
19.0
18.0
% ' _^
19.0
' \ <, ,' - '. v
19.0
17.0
5 '•• ""' -.^ 1 -A "•;,••*
; , / - ซ ff.e -
25.0
-v';v.;Ot
17.0
20.0
20.0
15.0
18.0
-'*(•> "v'v, ,'!
17.0
20.0
21.0
19.0
18.0
20.0
' \
33.0
18.0
18.0
19.0

22.0
19.0
19.0
19.0
18.0
21.0
21.0
27.0
36.6 ;
+ .• ' •."
15.0
20.0
18.0

17.0
20.0

Res. 3
17.0
19.0
17.0
,,'r:^'
18.0
1 , V ' , • "c
17.0
15.0
-. , f\'< •-"'•,- '
* * -* " ^ "-" '\
25.0

17.0
20.0
22.0
17.0
18.0

18.0
20.0
18.0
18.0
18.0
18.0

37.0
18.0
18.0
20.0
, "- - \ ,
23.0
20.0
19.0
16.0
18.0
22.0
22.0
23.0
34.0 .

15.0
20.0
17.0

16.0
20.0
No data submitted
Insufficient
data
X 3
Exper.
Sigma
1.15
1.15
1.00
' ^
0.58

1.53
1.53

,<''•)'
2.89
''' '' ' ' ' s
1.73
0.58
1.53
1.15
0.58

1.00
1.15
1.53
0.58
0.58
1.15
"'* V ' '
2.31
0.58
1.15
1.00
^1
1.53
0.58
1.15
2.08
0.00
1.00
1.00
2.31
2.65
•>' A •
0.58
0.58
0.58

1.00
0.58
Rnganal
(R + SR)
0.236
0.236
0.236

0.118

0.354
0.354
*"• -. "•••

0.591

0.354
0.118
0.354
0.236
0.118

0.236
0.236
0.354
0.118
0.118
0.236

0.473
0.118
0.236
0.236

0.354
0.118
0.236
0.473
0.000
0.236
0.236
0.473
0.691

0.118
0.118
0.118

0.236
0.118
Normalized deviation
Average
15.67
18.33
17.00

18.33

18.67
16.67
"^ ' "V* J' "=•> ,. '
\ " \ ' *''••''.'?
23.33
' ••• : •'•'•„ V -'/;
18.00
19.67
20.33
16.33
17.67

17.00
19.33
19.67
18.67
17.67
18.67
-•- ' ' ^
35.67
17.67
18.67
19.00

21.67
19.67
19.67
18.33
18.00
21.00
21.00
24.33
36.00

15.33
19.67
17.67

17.00
20.33
TAG SYMBOLS
Determined
to be an outlier
(grand-avg) (known) Tag
-0.97
-0.04
-0.50
:* ^"'C;;:/v:'s
-0.04
,. ;^.\"^"L::S
0.07
-0.62
••* wV{ s "-s ;:" ^ ^ •••'^ '
- cV x\- i% '""\ ->'-" ^*
1.69
\*.^'"-.tV>'{\
-0.16
0.42
0.65
-0.73
-0.27
' f ^-V /-'-
-0.50
0.30
0.42
0.07
-0.27
0.07
.' '''--"' };V;C'-.
S.96
-0.27
0.07
0.19
""'••,' ;
1.11
0.42
0.42
-0.04
-0.16
0.88
0.88
2.04
6.08
/•<-'_
-1.08
0.42
-0.27

-0.50
0.65
tt s Above
JJ = Below
-1.50
-0.58
-1.04
^•'-: oV-'
-0.58
'>->;^'";v. s*~""
-0.46
-1.15
\ •}"--^^' ^ .r ;; \
r'""" "l^*** ****-' * ' '
1.15
V; '^T-V/V/;
-0.69
-0.12
0.12
-1.27
-0.81
- ' .-'&^.
-1.04
-0.23
-0.12
-0.46
-0.81
- v. , • ,
-1.04
0.12
control limit
control limit

-------


EMSL-LV
Performance Evaluation: Blind-B, 18-Oct-1994
33/44
Cesium-134
Lab
DO
DS
DT
DZ
E
EB
EL
EO
BRV
EX
FF
FJ
FL
FNT
FU
FZ
GE
GI
GQ
GT
GZ
ffl
HK
HL
HP
HX
I
1C
m
._ ,.
J
JE
JG
JN
JQ
JS
JX
JY
K
KE
KT
KX
L
LF
• =
0 9
Res. 1
25.0
• \ ; •-""^
18.0
17.0
17.0
19.0
18.0
Res. 2
16.0
^>i:'-r~\ '• ,^'
21.0
18.0
18.0
18.0
20.0
Res. 3
15.0

19.0
19.0
19.0
18.0
19.0
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
5.51

1.53
1.00
1.00
0.58
1.00
1.345
v''"'' *
0.354
0.236
0.236
0.118
0.236
;\,^^V^:f;t^^ny^- ^ • - '• ' '/.<;->.'
21.0

19.0
18.0
"'\ """ " " ^ " "•VT^ s
19.0
19.0
16.0
18.0
17.0


x
19.0
18.0
18.0

18.0
20.0

17.0
17.0
16.0


18.0

19.0
19.0
• ฐ
*
20.0
20.0
19.0
	 17.0
r-> ;\. \ „, ,<
18.0
_ 19.0 	
ฐ •. -, ^ *. \- X
18.0
17.0
17.0
18.0
18.0
*
•
s
18.0
18.0
17.0
s -.
21.0
21.0
\ ^f; \; ^;;v
18.0
18.0
17.0
•*

18.0
"•
21.0
16.0
s
'' \
21.0
18.0
18.0
20.0

19.0
19.0
, * "• v
18.0
18.0
18.0
17.0
18.0

A

18.0
18.0
18.0
N
22.0
23.0
:f-v"'-
17.0
17.0
14.0


17.0

20.0
16.0


19.0
18.0
19.0
No data submitted
Insufficient
data
X s
2^08

0.58
0.58

0.58
1.00
1.00
0.58
0.58



0.58
0.00
0.58

2.08
1.53
"•
0.58
0.58
1.53

.-. . V. ..,^;': '<-.
0.58

1.00
1.73


1.00
1.15
0.58
0.473

0.118
0.118
/\\;
0.118
0.236
0.236
0.118
0.118



0.118
0.000
0.118

0.473
0.354

0.118
0.118
0.354


0.118

0.236
0.354


0.236
0.236
0.118
% 18.67_ ^
/" %" \" s *- v-\" x ^ ^U^I" ^ ^ *" v
19.33
18.00
18.00
18.33
19.00
•• s, % , " " s v ^ <•• ^ " \"
'* V"l9.33 '''''
; - ^-V'vW i,-,,v&'."> { '
18.67
18.67
-,s\ ."C ^/> -V
18.33
18.00
17.00
17.67
17.67

s s

18.33
18.00
17.67

20.33
21.33
~ • " '' ' ','-* ~\s' - f*&?
17.33
17.33
15.67

: \' ''%
17.67
•' - -'
20.00
17.00
s-
V
20.00
18.67
18.67
TAG SYMBOLS
Determined
to be an
outlier
0.07
-^it^^vy
0.30
-0.16
-0.16
-0.04
0.19
:K-"^
0.30
^ "t"" l " * •-
0.07
0.07
•\ - ; \o 5-1'^ ! \ .
-0.04
-0.16
-0.50
-0.27
-0.27
s
^ \

-0.04
-0.16
-0.27

0.65
1.00
, fXV>!X\Sv ,' \l "-'
-0.39
-0.39
-0.97


-0.27
.
0.54
-0.50
" -

0.54
0.07
0.07
ft = Above
$ s Below
-0.46
Z< X^< !'".•*•
-0.23
-0.69
-0.69
-0.58
-0.35
;i:';;/; >;ซ*,
-0.23
',Vt-^ - -• '
-0.46
-0.46
's'''*^ , .,: •"
-0.58
-0.69
-1.04
-0.81
-0.81
• "
*
ซ
-0.58
-0.69
-0.81
•
0.12
0.46
^•-^v V,
-0.92
-0.92
-1.50
~' '' " *
' - •
-0.81
'V - •
0.00
-1.04
*
ซ
0.00
-0.46
-0.46
control limit
control limit

-------
34/44
EMSL-LV Performance Evaluation: Blind-B, lg-Oct-1994
Cesium-134
Lab
JDG
* •-J.J.M'' s
LR
LT
M
MA
MP
MQ
MV
MV
N •
NA
NH
NJ
NK
NO
O
OF
OS
OX
OY
P
PA
PB
PG
PI
PM
PR
PV
PW
Q
QC
QJ
QP
QQ
QT
QU
QW
QX
QZ
RC
RD
Res. 1
',.'"' y * "'*
•> f s' •• s ,,'•'••
29.0
17.0
20.0
19.0
15.0
17.0
14.0
. '' 34% '
^
' ^ -.'" " •• '
18.0
20.0
18.0
46.0
19.0


20.0
*
22.0
17.0
16.0
' , _ ; ' '!
16.0
18.0
17.0
- -,-""' --\\' '
17.0
20.0

17.0


21.0
17.0
* " v J4- j S "" '^
Res. 2 Res. 3
"'0>?":-: ?V,.
,.'. <•*%? *^~ , '^ ?•' '•• •• "^
31.0
17.0
21.0
18.0
17.0
17.0
15.0
;V;32La\t;^
''•"'"' - \ / % *" * ^ "\ * w
18.0
17.0
18.0
'* ; 46.0 -^.">
• ,^' - - - -? ,v •- .v ^
19.0

! • - /'-v'
22.0
^
21.0
17.0
18.0
-;- ' I' -KvV'
16.0
17.0
18.0
, ;-\'v" "'; ,V- /'
17.0
15.0
17.0


21.0
16.0
:&\-^[\ v,%-;i>
,^\; 	
^ ^ '^ ••
24.0
17.0
22.0
18.0
15.0
18.0
16.0
38,0
'^<\>,-
17.0
18.0
17.0
W$'.
19.0


20.0

20.0
17.0
17.0
V' "''
20.0
16.0
18.0
:-:>;' '';
16.0
18.0
17.0


21.0
16.0
• = No data submitted
0 =
Insufficient
data
x =
Exper.
Sigma
-. JvJ -.
*% 1. ' " %
3.61
0.00
1.00
0.58
1.15
0.58
1.00
, r lOO
'"- ,;
0.58
1.53
0.58
; too
0.00
t •• "•

1.15

1.00
0.00
1.00
- '-,'• '..
2.31
1.00
0.58

0.58
2.52
0.00


0.00
0.58
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag


0.827
0.000
0.236
0.118
0.236
0.118
0.236
0;236

0.118
0.354
0.118
0.236
0.000


0.236

0.236
0.000
0.236

0.473
0.236
0.118

0.118
0.591
0.000


0.000
0.118
, , ;'. /.'}< .
s •• ' •• * ""* '•-'^ %, '
28.00
17.00
21.00
18.33
15.67
17.33
15.00
; ,; ^33.00
'V, ' - \ - ' ,.Vj
17.67
18.33
17.67
. 46,00
'- '• '•'•'^ .]•'• '• '• t '-'•'• '• v '• '• '•
19.00
/V \;:

20.67

21.00
17.00
17.00
•:• ป \'. v -/ }
17.33
17.00
17.67

16.67
17.67
17.00


21.00
16.33
TAG SYMBOLS
Determined
to be an
outlier
' > V ' ^ ' ,~- -'y.
\ * * ^J^' ' <•' f-.^y^
3.31
-0.50
0.88
-0.04
-0.97
-0.39
-1.20
,,xR04V-,-:
•.! ••' •- •••. ' ^ -
-0.27
-0.04
-0.27
x'<^ ;^
0.19
<• '• "', ^-'/'V ;'
11 v^
- '-' .. -' V'--
0.77

0.88
-0.50
-0.50
- / * ',' • . ," -, -
-0.39
-0.50
-0.27

-0.62
-0.27
-0.50


0.88
-0.73
ft s Above
It = Below
•>•, ^ 's , ''% % V*' '
.V" *•;%*'' 0
* JH •, V t't' •. '' '•.-••••,
-\ •* p"' ' <;"'' ^'*---^ ' ^m ^ '•
J;*'\\ss;-'s>s>'' vป '*•'• v
2.77 	
-1.04
0.35
-0.58
-1.50
-0.92
-1.73
4;50. X
•, ' • ' *
-0.81
-0.58
-0.81
••O ftl '' •y'1''
-0.35
;-"*'^*;v.:i
•ซ/ •' ;'"*!?'
--' , -'ป ''-*
0.23
^.. ;- ^ -
0.35
-1.04
-1.04
x; : /'';.{,-
-0.92
-1.04
-0.81
.--,/-' •' -
-1.15
-0.81
-1.04
' ' ''/~*''
\ *
0.35
-1.27
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
35/44 1
Cesium-134
Lab
RF
RG
RJ
RK
RL
RM
RP:
-RR*
RV
RZ
S
sc
SD
SF
SI
SL
SM
SN
SO
SR
88
ST
SW
SX
SZ
T
TD
TE
TH
TI
TL
TN
TQ
TS
"'TY-
u
UA
UE
UG
UK
UN
UP
*Dtf
uw
UY
• =
0 s
Res. 1
Res. 2
V-^.N'^'^^lfe^:
\ \
22.0
^xC.^'V? ,'"Y^
I ^ ' •'"•',• -f
18.0
18.0
16.0
22.0
17.0
22.0
"*'' * o V:-™- ^
15.0
19.0
18.0
- v* v ^
18.0
18.0
16.0
18.0
18.0
19.0
18.0
21.0
<
18.0
17.0
~!' '^ '•;-'';;!>
19.0
20.0
- ,>-,'—-
12.0
19.0
17.0
19.0
21.0
- • ' - S",\ ' " '''
20.0
^ •. " "" ** ^
A "^ C '* "" s v "

X ' v^f •&* *" "•>
17.0
18.0
15.0
16.0
17.0
19.0
,- v^A^Y ''
16.0
19.0
r*x:S;i;;:>i
19.0
19.0
17.0

18.0
17.0
17.0
19.0
17.0
18,0
19.0
21.0
' .- S" -x^>
17.0
18.0
^\ "• \*\^; " " -r^
21.0
21.0
\ " ^ t"' s ^
27.0
18.0
17.0
20.0
19.0
Res. 3
:1ฃfk
hf":^';" "
18.0
""•.-. -••.'''•••
?/-- ^-^\';
:^o27:o^'
19.0
18.0
18.0
25.0
17.0
19.0
\i" "• % s ^ O%
17.0
20.0
/^HV:~ r
22.0
20.0
17.0

20.0
18.0
17.0
18.0
18.0
20.0
18.0
15.0
*•'••
16.0
15.0

20.0
20.0

19.0
18.0
19.0
19.0
18.0
No data submitted
Insufficient
data
x =
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
\X^v,: ,

2.00

\ -
-7,3.46- - .
1.00
0.00
1.53
4.58
0.00
1.73

1.00
2.65 .

3.51
0.58
0.58

1.15
0.58
0.58
0.58
0.58
1.00
0.58
3.46
„
1.00
1.53

1.00
0.58

7.51
0.58
1.15
0.58
1.53
-: ,V'i"''
- ซ -1
0.473
••" x"* ^ ••

0.709
0.236
0.000
0.354
1.120
0.000
0.354

0.236
0.591
'"• . >'
0.827
0.118
0.118
-1-
0.236
0.118
0.118
0.118
0.118
0.236
0.118
0.709

0.236
0.354

0.236
0.118

2.470
0.118
0.236
0.118
0.354
tX,Ui.^xv^'Xf*
;:-;\-;*;/V. u^^
VLi-'^x)^^^
20.00
!''XV r^''l\V-:Vf'-'^
- ,\; ^^j'-'r^s '^;,,\
, ' s-31.00:^;r^
18.00
18.00
16.33
21.00
17.00
20.00
- *,--.> ;:*vV->\Vx?/
17.00
18.00
" "v^^?^^*?3?
18.67
19.33
17.33
- ^"ซ "" x
18.67
17.67
16.67
18.33
17.67
19.00
18.33
19.00
, ^ "x_x
17.00
16.67
'ฐ '7 •ป• -x' ;- x.-.
20.00
s \ ^
20.33
xU'^ ;J:"\\-^-
19.33
18.33
	 ^17.67
19.33
19.33
TAG SYMBOLS
Determined to
be an
outlier
:;fel|ilrS|iivi;%:"
• , s';-*? -f ;!f; fj\- ffi ^ • - : -, x-j -s, -
^'^:i:?;^:
0.54
*''''? X% ฐ'C*'\-
--> '^P^iVs' :-
A35^^>\
-0.16
-0.16
-0.73
0.88
-0.50
0.54
iVV^'v--*.
-0.50
-0.16
-7^^:^":
0.07
0.30
-0.39
v -
0.07
-0.27
-0.62
-0.04
-0.27
0.19
-0.04
0.19
X,' ,^
-0.50
-0.62

0.54

0.65
* ' * < ~' ' ' ' '
0.30
-0.04
-0.27
o!so
0.30
tt s Above
& = Below
^.\':': •-'%•• *' '
o.po
CrS';^:*'
v " ,Vv'-^; -'-"• ''*
:- 3:81.- xVx; -:
-0.69
-0.69
-1.27
0.35
-1.04
0.00
11 X*.^s i ^.,,
-1.04
-0.69
Ix^y^V''"
-0.46
-0.23
-0.92
AV, V \ V. ^
-0.46
-0.81
-1.15
-0.58
-0.81
-0.35
-0.58
-0.35
" *Vs X\t x
-1.04
-1.15
-:ฐ '"'" 1- * '•
0.00
„:. ' ; \ -•
0.12
;!- ; '• *'
-0.23
-0.58
x,:ฐA81^ ~.ซ
-0.23
-0.23
control limit
control limit

-------
36/44 EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cesium-134
Lab Res. 1 Res. 2
VC 19.0 19.0
VG 16.0 17.0
Vl "- ' ,- "' '*'"'. *<•'*'
VjT-'. 'v' 'Vr"^;::ซ'i''
• VM '•;,' . . :. . _:; -,;-;'
- _—. '•>'''•*,,' * - - ( :'t>\~\ '..',,
' VN ";' -,":' - "' """" ' "yป- - ''^^ "\
VO 18.0 19.0
'-.,* "• •••••"• „* ^ ••'•'•••'_, O' :':';'• ,..'••.' y •ฃ,*•
"VQ" '-•.<• J'""ฐ ^ <'"/-•ป>*• ,\ >f :;;,'
VT 14.0 17.0
VU 17.0 17.0
•• x , r '•> .-
W 18.0 18.0
X 17.0 16.0

Exper. Rng anal
Res. 3 Sigma (R + SR)
19.0 0.00 0.000
18.0 1.00 0.236
*!"" ,' '"' - ' *, ''•
\V.\fe '^-" ;v; • > / ' - \ ;
,* , ^ *< * ^ ^ ' \ ' •• '*• i *
\*,\^ ,-\-\' s-'^r '•>, "','-' - -, -
;*,*\">: " •. 'i>""f:f<-,\" 	 <"'•/ • ..> ' " ' • •'.. ' •• •:. "'
19.0 0.58 0.118
""" ^'"-•••i^"'* " T " !^--AJ1 s, '"* * '"'"' ' '' •."'•<•'••- '' \ '• "•
-*f* $$" S**' - S\V-*' -' >"
20.0 3.00 0.709
17.0 0.00 0.000
V-, ,v"- '-'\- <*\ -<•.,-• • ' ป,* • ' '*
17.0 0.58 0.118
17.0 0.58 0.118

Normalized deviation
Average (grand-avg) (known)
19.00 0.19 -0.35
17.00 -0.50 -1.04
'•• '-'-' .. - ''V '" ป' "-"•-- ''-T-v^
•• *-''•' :-: ^" "*?'-."' >5'; /"• ':" ;':|ฐfc ^
>- - ,j\ '^'-' - ~:"'"~ *- - -. '' ' r"*<.-'J!'- -v-'
", , * ,'J " S '** -'*',', ~ ,~ ', 1' "•• - V"- C^';'' ">ป"'- -\s'
;- ','•"".". -1-"' ••••>;,'"., ซ' 'ป'<;'V " ' "--v *x s '••• <* 5
18.67 0.07 -0.46
••i -. "• fy- ..^ '•','• s ^WAS^^-, A / ^wjs w ^ -.^AW ^ ^.^ ^ %^V.%M. s ^\
\-' " A"- ' ,-""" ' " "; '-. , - '•.'"-'- " ^
17.00 -0.50 -1.04
17.00 -0.50 -1.04
•' . ' ,-'-"• •. \ *-' '• '•.''*',• ~- "V ^'-: I. ~'; '! \C
17.67 -0.27 -0^81
16.67 -0.62 -1.15

Tag


>/>•:?
ง:t
,"•• ••
\ X "•'•• {
, \ (ง,,,,,,,

*"•*
\ *'


^ ,s


Data sorted by Laboratory Average
Average Tag
15.00
15.33
15.67
15.67
15.67
16.33
16.33
16.33
16.67
16.67
16.67
16.67
16.67
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
17.00
• = No data submitted
0 = Insufficient data
Lab Average Tag
MV 17.33
DD 17.33
MP 17.33
JG 17.33
A 17.33
SC 17.67
QZ 17.67
BA 17.67
X 17.67
TS 17.67
T 17.67
QJ 17.67
AL 17.67
VU 17.67
VT 17.67
VG 17.67
TQ 17.67
SM 17.67
SF 17.67
QT 17.67
PW 17.67
PM 18.00
PI 18.00
LT 18.00
K 18.00
GE 18.00
DL 18.00
BH 18.00
AF 18.00
TAG SYMBOLS
Lab Average Tag
ST 18.00
PV 18.33
MQ 18.33
JE 18.33
J 18.33
W 18.33
UP 18.33
TE 18.33
SZ 18.33
QP 18.33
Q 18.33
NK 18.33
NH 18.67
JS 18.67
HP 18.67
GQ 18.67
GI 18.67
DG 18.67
C 18.67
BN 18.67
BC 18.67
SN 18.67
S 18.67
RZ 18.67
HL 19.00
FZ 19.00
E 19.00
DZ 19.00
CP 19.00
IT s Above control
x = Determined to be an outlier U = Below control
Lab
AU
UN
TI
TD
NJ
MA
HK
FU
EB
CO
AI
AE
VO
sx
SR
LF
L
FL
F J
DO
CA
BO
BM
AK
VC
TL
TH
O
EL
limit
limit

-------
EMSL-LV Performance Evaluation: Blind-B,
Cesium- 134


18-Oct-1994 37/44 I

Data sorted by Laboratory Average
Average Tag
19.00
19.33
19.33
19.33
19.33
19.33
19.33
19.33
19.67
19.67
19.67
19.67
19.67
% responding labs
Lab
CE
UY
UW
UK
ss
EX
DT
BK
DE
CM
CK
BL
AW

Average Tag Lab
20.00 U
20.00 SI
20.00 RM
20.00 KX
20.00 JY
20.33 UE
20.33 I
20.33 DM
20.33 AZ
20.67 P
21.00 SD
21.00 QX
21.00 PB
Frequency distribution
Average Tag Lab
21.00 M
21.00 CS
21.00 CQ
21.33 1C
21.67 CJ
23.33 AP
24.33 CX
28.00 LR
31.00 x RV
33.00 x MY
35.67 x BW
36.00 x D
46.00 x NO


m.
IU' -----------
n.
ฐ -6 ' -4



1
Illl,
•Illlf .
_• IIIIHiil 	
-2 T I ' +2



+4 ' 4
Normalized deviation of the mean from the known value
% responding labs

ซ -----------

10" -----------

-6 -4






Frequency distribution



IiLii.
..Illlllll 	





_ _ - •ป
-2 0 +2 +4 +6
Normalized deviation of the mean from the grand average
• H No data submitted
0 = Insufficient data


TAG SYMBOLS
x = Determined to be an outlier
ft = Above control limit
•li = Below control limit

-------
                 EMSL-LV Performance Evaluation: Blind-B,  18-Oct-1994
                                  38/44
Cesium-137                         Statistical Summary                      193 Participants
The known value of this nuclide is 39.0 pCi/1 with an expected precision of 5.0; the control limits
are 30.3 to 47.7; the warning regions are 30.3 to 33.2 and 44.8 to 47.7
66(34.2 %) Failed to respond .
6(3.1 %) Outliers **
4(2.1 %) Out of control
     but not an outlier


         Statistic
                106(54.9 %) Within all limits
Respondents
••• 11 (5.7 %) In warning zone
            but within control


               Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
     42.76
      6.97
     48.60
     16.30
      9.63
      0.54
     41.67
      6.84
      0.38
     Grand Avg 41.73
                  2.66
                  7.06
                  6.37
                  7.01
                  1.03
                 41.33
                  5.98
                  0.88
11 (8.7 %) More than 3 norm. S.D.

1O(7.9 %) Between 2 and 3 norm. S.D. •
              8(53.5 %) Within 1 norm. S.D.
                           of known value
     38(29.9 %) Between 1 and 2 norm. S.D.

-------
397
44
^1
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cesium-137
Lab
A
AE
AF
AH
AI
AJ
AK
AL
AO
AP
Alt
AU
AW
AZ
BA
BC
BG
BH
BK
BL
BM
BN
BO
B8
BW
C
CA
CE
C<3
CJ
CK
CM
CO
CP
CQ
CS
CX
D
DB
DD
DE
DG
BJ
DL
DM
Res. 1
36.0
39.0
39.0
41.0
'- .' -~- / s
43.0
41.0
45.0
•;-->- ." • '-"
39.0
48.0
40.0
41.0
40.0
410
43.0
41.0
44.0
44.0
42.0
38.0
69.6
40.0
40.0
42.0

39.0
45.0
45.0
49.0
40.0
46.0
48.0
45.0
90.0

35.0
39.0
43.0
37.0
43.0
Res. 2
36.0
41.0
41.0
44.0
f " ' S^s ^
42.0
44.0
/* \ "" ' ""**"
38.0
:' Vx*'~'~"'>
42.0
45.0
42.0
38.0
42.0
44.0
42.0
40.0
42.0
42.0
41.0
, i f
68.0
39.0
43.0
40.0
" ' V
43.0
44.0
41.0
50.0
40.0
48.0
48.0
42.0
77.0

35.0
40.0
44.0
40.0
43.0
Res. 3
40.0
42.0
42.0
42.0
V* ---'-;; I-'*-;' ',>
43.0
41.0
41.0
!-',""~ ",^'V"*' \
40.0
44.0
43.0
37.0
42.0
: ; mo
43.0
42.0
40.0
43.0
43.0
45.0
• . v- " !-' ' , ' '
40.0
43.0
44.0
 '" ">',
40.33
45.67
41.67
38.67
. 41.33
5167
43.33
41.67
41.33
43.00
42.33
41.33
68.67 ,%
39.67
42.00
42.00
" :, ,' <~<
41.67
45.67
41.67
48.67
40.00
47.67
48.00
47.00
8133

35.00
40.00
43.00
39.00
42.00
TAG SYMBOLS
Determined to
be an
outlier
Normalized deviation
(grand-avg) (known) Tag
-1.52
-0.37
^-0.37 	
0.21
^\I\-'"1;'-1 --<>••:;
0.32
0.09
-0.14
:fV,f';v' >- *
-0.48
1.36
-0.02
-1.06
-0.14
^>;3,44-;':-'
0.55
-0.02
-0.14
0.44
0.21
-0.14
(/i;^ฃ
-0.72
0.09
0.09
'''-T,/.f".f'-X
-0.02
1.36
-0.02
2.40
-0.60
2.06
2.17
1.82
13.72

-2.33
-0.60
0.44
--A- : -X",.~ • <\
-0.95
0.09
ft = Above
U = Below
-0.58
0.58
0.58
1.15
'-''-- ;'v<,.ป'\:i
1.27
1.04
", ' f\'t s\ ,
'v >-J- - •*
0.81
"'"'; '!"1- '.* .
0.46
2.31
0.92
-0.12
0.81
y!'i':39'; X
1.50
0.92
0.81
1.39
1.15
0.81
10.28 x
0.23
1.04
104
{> 'T. \ „*,"',
0.92
2.31
0.92
3.35
0.35
3.00
3.12
2.77
14.66 x
'.-' -' ปV
-1.39
0.35
139
^ '-, - -- --, '* ••
0.00
1.04
control limit
control limit

-------
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
40/44
Cesium-137
Lab
DO
DS
DT
DZ
E
EB
EL
EO
ER
EV
EX
FF"
FJ
FL
SN
FU
FZ
GE
GI
GQ
GT
GZ
m
HK
HL
HP
fiX
I
1C

iij
IE
J
JE
JG
JN
JQ
JS
JX
JY
K
KE
KT
KX
L
LF
Real
46.0
49.0
35.0
41.0
46.0
39.0
• \ ..X"
/-"~ , -S!.-T-
42.0
44.0
41.0
\ , 7;rv;^M^
44.0
46.0
40.0
40.0
39.0

' \, '

43.0
44.0
45.0

41.0
42.0


" + ^'-^ ••
41.0
40.0
42.0


41.0

44.0
39.0
^

38.0
38.0
39.0
Res. 2
41.0
46.0
35.0
44.0
47.0
. ,^,43-.cL,,.,, .,
- :;,;|ง^#
: '\>\^^t
38.0
40.0
42.0
r;;^7y:-^>^^
39.0
45.0
40.0
42.0
......I!:.0.,,
-. C-* •, -. -.^ - ^ \ '•'.'.
\ s ^ -.-.^ s"1""1 '""- •""" ^ "•
:-\!vr"v\\' •

43.0
44.0
46.0

42.0
44.0
••V •. % •.-" x Vi"''1 \ 4*
"^ "'' %"" SO 0* / s * ^C"
>C ^-iv ^^ ^^V* N ^•"•''
42.0
40.0
42.0

-
40.0

44.0
35.0
- -
•j v
40.0
39.0
42.0
Res. 3
41.0
38.0
35.0
45.0
47.0
42.0
?;" -!>Xk-V-
;"-^;V
39.0
40.0
41.0
X^'-'V
3S.O
49.0
37.0
42.0
38.0
\ v *v %
> '--\ - !
- ^ -1" ,'
43.0
44.0
45.0

40.0
43.0
% s ^ ^ %
" ' V"-* "*
1\\\- ;-- ,'o \
42.0
40.0
44.0


39.0

41.0
39.0
•-
.
42.0
38.0
39.0
• = No data submitted
0 s
Insufficient
data
x =
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
2.89
5.69
0.00
2.08
0.58
2.08


2.08
2.31
0.58

3.21
2.08
1.73 .
1.15
1.53



0.00
0.00
0.58

1.00
1.00



0.58
0.00
1.15


1.00

1.73
2.31


2.00
0.58
1.73
0.591
1.570
0.000
0.473
0.118
0.473


0.473
0.473
0.118
c;ฐ-'j
0.709
0.473
0.354
0.236
0.354

s

0.000
0.000
0.118

0.236
0.236



0.118
0.000
0.236


0.236

0.354
0.473

<
0.473
0.118
0.354
42.67
o-T-i' „• !\^-x^- !
44.33
35.00
43.33
46.67
41.33
^•'-;%\\^
• , \-;-~ ^v - TO
39.67
41.33
41.33
.._ -^v^^~
40.33
46.67
39.00
41.33
39.33
•-'":; ;^ ;t\'-!3:
\ -' o-'V'"-'1 ''- *
•0 ' •/. ;:A5~?'^;:V
43.00
44.00
45.33

41.00
43.00
^ % ••'•; i- l _% •"•* A^-V •• s w
' -" ioซ - v " " ^t;A- ^ \ ^.
-,;- ^: ^xg;:4r
41.67
40.00
42.67

* N
40.00
>
43.00
37.67
>

40.00
38.33
40.00
TAG SYMBOLS
Determined
to be an
outlier
-;;-fl^;
0.90
-2.33
0.55
1.71
-0.14
^'-"r-'-vk?:'"
^y..'^.^^'
-0.72
-0.14
-0.14
'^^^'7^"
-0.48
1.71
-0.95
-0.14
_:0.83_ ^

''K'^iK "V '
*'- "ffCV{f ",;-*';-:' -"\ N,-;
0.44
0.79
1.25

-0.25
0.44
w. s w ^^ "" ^ " l" ^ ^
5' ^ -r*s ..-Si. - \ x ' ' \
>*~ฐfM -\ ^f~- x-"
-0.02
-0.60
0.32
*

-0.60

0.44
-1.41
\ \\ \ S
•> x "* "
-0.60
-1.18
-0.60
ft = Above
& = Below
x 1;27
1.85
-1.39
1.50
2.66
0.81 	
,! tt'v' >"' *' '
••'•Sv* .ซ- •
0.23
Vc'x- > > • *
0.81
0.81
•ป \s •• %1" A ^
0.46
2.66
0.00
0.81
0.12
• ":? ""<:•*;" ';•*"'
-\,V,\-> ,v '
- ' X : " - •
1.39
1.73
2.19
•
0.69
1.39
^ <•„..••;• ,, w. "•."••'.'• •>"
v 'i-% ^ "" ^"*" -
•VK^ VVx
0.92
0.35
1.27
•
*
0.35
*
1.39
-0.46
. *
s s% *
0.35
-0.23
0.35
control limit
control limit

-------
417
44
Cesium-137
Lab Res. 1
LCJ
LL
LR
LT
M
MA
MP
MQ
MV
MY
N '
NA
NH
NJ
NK
NO
NT
0
OF
OS

OX
OY
P

PA
PB
PG
PI
PM
PQ
PR
PV
PW
Q
QC
QJ
QP
QQ
QT
QU
QW
QX
QZ

KG
RD
RE
"T'V*?* "X*
•>' '.*'*" '-V'
40.0
43.0
40.0
45.0
35.0
41.0
43.0
81.0

'" , ' •' ; ''
44.0
41.0
41.0
22^
t .. ••
44.0
w, /"" ' ' ''''
- ! ' ," ' /•

,- ' ->-.-.
.
49.0

11 •.'"'*
41.0

42.0
41.0

' - •
46.0
40.0
38.0
,-•
40.0
42.0

40.0


49.0
40.0


'? '*
*• '• ' , '" ' '\ <'-
EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Res. 2
yxxV'^-^:^^ "" v
* •• < "*%*'• ., ^ ^* v"'*"*
=- "/p^/t1
41.0
41.0
41.0
46.0
39.0
40.0
47.0
\ "::'$$ฃ

'---"X^v
43.0
40.0
40.0
23.0
r '
44.0
. ~ . ', >;- ' -:
- _ •' ~'V;\:-
"• ' , ,-. -. •• X '•> v ^ 0 ..
;/";':;> Vx-
^\ - , ff z* ,"
46.0


43.0
, ' , "V';\-
41.0
39.0


45.0
40.0
39.0
-, ' '•
41.0
43.0

40.0

" "'-
49.0
39.0

t,"' -" '" : '•
ฃ :-]?•ฃ.*
i/,^v.,\\r
Res. 3
g^;^V>!;":j
4^-^V'-. ~;-'V'
39.0
40.0
41.0
44.0
37.0
41.0
38.0
'••X '\- •• --^f •.
\* "" **> % ^ % O jLjv * '
-.-•<.' ,. ••
"••'•." V^s " "-
44.0
42.0
42.0
23.0
- , ,,.
44.0
; ;,"';^ , ^ , :
-* ^-;;;H/; <~',\*
""•.•• f$ "• \^(~- •" 0 ^ •.
''i^x^v -V?v,;
•,-"'- '"'' ' >
42.0
i '
40.0
39.0
s > .
;- ' ' '-* '' ;':
37.0
40.0
41.0

41.0
44.0
*• r
40.0
, '..

50.0
39.0

^T^ ';"'• "'," \ ^
?'"<** r-^; '''•*,
VV^'.'v.-V
• = No data submitted
0 3
Insufficient
data
X s
Exper.
Sigma
v "t ""
S-v^,.' ^ ,
1.00
1.53
0.58
1.00
2.00
0.58
4.51
^-0.58
v ' ^

0.58
1.00
1.00
:0,58

0.00

-. -. * \
* f *• f '"• -.
,';;-',-, ' '

4.04

'•.*"•• ^ '
1.00

1.00
1.15
•:;;V-!

4.93
0.00
1.53

0.58
1.00

0.00
*
„
0.58
0.58


^ -'v, \.. '/
'-'';"'- "• ~
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
j ""•
,
0.236
0.354
0.118
0.236
0.473
0.118
1.120
0.118


0.118
0.236
0.236
6.118

0.000



*

0.945


0.236

0.236
0.236


1.120
0.000
0.354

0.118
0.236

0.000


0.118
0.118




,v \. ',/••'; '~\'*^x''
• , . **]•[* - - •/;,;
40.00
41.33
40.67
45.00
37.00
40.67
42.67
.' '^LSSC ' '•
' '." ' "• / -.* 0

43.67
41.00
41.00
. 22.67 >

44.00
* -' - -~ ," •-' -\~
S. -.} /

^ v -. __ \%";f/ 0"* t ~~ f"\
_ ', ^ ""^ -. ^ : ' '*•
45.33


42.00

41.00
39.67

- < _
42.67
40.00
39.33

40.67
43.00

40.00


49.33
39.33

f * . . . ^ • •-, v ' ,,
'••''/~'^i-,^'
1-\'.,-*-';< \ 'i<:...6
TAG SYMBOLS
Determined
to be an
outlier
v,*T>/;,lt^<^
!>V':X y^^l';
-0.60
-0.14
-0.37
1.13
-1.64
-0.37
0.32
-; 13*72 v;/;,:
. ,- " ',--' >'••
' ! <*' JKX\; •"•

0.67
-0.25
-0.25
-6.60
1 ^ N *"'•• : S
0.79
"•"" KO ^v ^ '-. -. "''

; *• ^ ' *" * *•••
^Vv'.'vi/51"'^""
- :- -,-;;-- ': ,
1.25

v '-- "" '' : ••
0.09
;/""-: •' :--';:
-0.25
-0.72
'' •• •• %-.'•'
. ""MV,"
0.32
-0.60
-0.83

-0.37
0.44

-0.60
-. • " '--

2.63
-0.83

•- >,/:•'. , '•*
;'.t<-"-ป l'--<;v; -'''/;'>
" ' ' :'"' "' '•?•'"' -""" '•>..
tt s Above
It = Below
^?''4^r:>^v
*/!{;'! v'* ป * 'V ^ -'•••"•

2.19

- ; - ^ •••••< -. - •
1.04
•.*.' ? 4k •>
0.69
0.23
-.; - :'"' x*'"
'"';."/';< '• "
1.27
0.35
0.12
->" - , , , ; ,# -
0.58
1.39
;',' ' '-" * '-
0.35
;f;' - '-/-•• '
.' • ' *
3.58 'It'
0.12

'-•-^-, : *
x *./'!' ^^ •ป '^ ^v'. '%
l^'i.l!!.,'.:*!...:..
control limit
control limit

-------

EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cesium-137
Lab
- Btfo
KG

RJ
RK
RL
RM

RP

RR
RV
RZ
S
sc
SD
SF
SI

''•' C3T
*$.K>MJ *
SM
SN
SO
SR
ss
ST
SW
sx
sz
T
TD
TE
TH
TI
TL
TN
TQ
TS
TY
U
UA
UE
UK
UN
UP
UQ
uw
UY
• 3
0 s
Res. 1
/*• "'-'.'<*ป'* '?t^~
";;<--;; iX;';'f

- ;--:;;-\

• •'• "-;V,
36.0

•~ ' - " %\ ~V- "

„' *"*• • ' ''•*"'••-'
^V- '7l,fe
39.0
40.0
41.0
40.0
39.0
43.0
-V- ; \ v

_-, * "-"^"^-v \^" "--'"'
39.0
39.0
- - ' ^r> $5^
37.0
41.0
40.0

42.0
41.0
41.0
44.0
45.0
46.0
42.0
43.0
',;.:*, ^
42.0
40.0

44.0

42.0
57.0
45.0
41.0
, .
42.0
41.0
Res. 2
i^r^-H^
'/: ii^'X '- *;''

x^^rt;"'' :* %
A-*'7'V:. V^
- s'l - -, ' - x-
38.0

- 0-~' v'f'-H

'"'-'-;>ป' x'^'-i';. -Y
•'•^,&:U
38.0
42.0
42.0
43.0
44.0
41.0

* s !; ~OY *• v*5s v'•''--::^^ x v\
^-"A^ s^, ^. ^ s^c-
38.0
39.0
v^1""^:-^''
36.0
44.0
44.0
\
43.0
42.0
42.0
45.0
43.0
46.0
44.0
43.0
;-V;'^:^X-V-^
39.0
41.0

42.0
••
43.0
42.0
44.0
40.0
v ^ " V
44.0
42.0
Res. 3
s. ":v ,
V - ^ '" -

% "s •• '
-?t^ ;•/. -
\sVซ s7s v-s
35.0

^voV ; ^

>-"V\;~'
:.ai.o
40.0
41.0
37.0
46.0
39.0
48.0

V. ^V, * O ''Is \
- " - :•
38.0
40.0
>/;V;^''
41.0
40.0
40.0

41.0
40.0
42.0
42.0
43.0
47.0
43.0
38.0
^ -' ! ^\
44.0
42.0
-
44.0

43.0
49.0
46.0
42.0

42.0
43.0
No data submitted
Insufficient
data
x =
Exper.
42/44
Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
•- ;>





1.53



•.•*
5.51
1.00
1.00
2.65
3.00
2.89
3.61



0.58
0.58

2.65
2.08
2.31

1.00
1.00
0.58
1.53
1.15
0.58
1.00
2.89

2.52
1.00

1.15

0.58
7.51
1.00
1.00

1.15
1.00

•




0.354




1.345
0.236
0.236
0.591
0.709
0.591
0.827


"• . • '
0.118
0.118

0.591
0.473
0.473

0.236
0.236
0.118
0.354
0.236
0.118
0.236
0.591

0.591
0.236

0.236

0.118
2.470
0.236
0.236

0.236
0.236
,N;vV'^?;:S
^ - .. N x v " s * \

•"';•->•? *cr>'V
>-""ฐ' '" Vv-5. ' ~ *
"T:- -.V ;V^;x>;H
36.33

' ' ' '-• -: - Wx;

,--- \-,, ' --<.'•> !>i
:-'-'c 74^67^4
39.00
41.00
40.00
43.00
40.67
44.00

W X^'ss ^s \ V '•''* *• •<" '*•.

38.33
39.33
\
38.00
41.67
41.33

42.00
41.00
41.67
43.67
43.67
46.33
43.00
41.33
,,^ ,-^<.-\--V -;-;-
41.67
41.00

43.33
_
42.67
49.33
45.00
41.00
<
42.67
42.00
TAG SYMBOLS
Determined
to be an
outlier
^r^S3
^•> -V; -'i,^^|

,I-"p^f;'-;^>;-
>:^r:"^l!i
;:y\-*^|"- '•'
"-1.87

^VYK™"' ':ฐ ~~

,s ci -\V--; '
v'iii4KV:^
-0.95
-0.25
-0.60
0.44
-0.37
0.79

5. ^ \ i \ •% '•V'5 s ^ NA ^t^'* ^ ~ ^
"^^V "" V^"N w
-1.18
-0.83
'^Vvx^.-v-^ "•* :- >;
-1.29
-0.02
-0.14
' X
0.09
-0.25
-0.02
0.67
0.67
1.59
0.44
-0.14
^j\\,-;-Vซ"!.Vv
-0.02
-0.25

0.55
v *
0.32
2.63
1.13
-0.25
v ,.,,„., ^~ ^
0.32
0.09
tt s Above
•li = Below
^'Cvv-^v--'1- •

* ' <- ^ s \ v •• " ' ••
tt-iV.vvr'-,* "
;(^S'*'>A
--, v x '" >'• - * -- .
-0.92

- -' x\ • •

• ' ;\' V •
I^k36 x
0.00
0.69
0.35
1.39
0.58
1.73

\i \%1> iXsXX.s---'' v A ••
s 1 -• - \"
-0.23
0.12
;-^v^f s.!f-
-0.35
0.92
0.81
•
1.04
0.69
0.92
1.62
1.62
2.54
1.39
0.81
x<'->ox-V •-
0.92
0.69
•
1.50
•
1.27
3.58 tt
2.08
0.69
v v v \
1.27
1.04
control limit
control limit

-------
43/44 EMSL-LV Performance Evaluation: Blind-B, 18-Oct-1994
Cesium-137
Lab Res. 1 Res. 2
VC 37.0 41.0
VG 42.0 38.0
/vi. j ,J;v:,,,;>\V^^
Vdl ;" • '• ""> '" - < •-. 'f'-'f ^
,VM ' ', <- , /'-'v ;:'V—
-VN >'-' '< - -'<^/;< hV
VO 45.0 44.0
VQ - , ' v..v
VT 32.0 38.0
VU 41.0 40.0
-vs.',/ •• ' /•• ;" :
W 43.0 42.0
X 39.0 38.0

Exper. Rng anal
Res. 3 Sigma (R + SR)
38.0 2.08 0.473
42.0 2.31 0.473
?Hฃ -V^'-':-;:--", '. '•
"" "' " ' "* * '" """r *'* *
"• v ••'''' '* ' , ^ •. ^
,- V- ^" ; ^ '" '.-.-. ' , , f ••
45.0 0.58 0.118
*• •> x -. -. ".,
44.0 6.00 1.795
40.0 0.58 0.118
",-"<. • - *
42.0 0.58 0.118
40.0 1.00 0.236

Normalized deviation
Average (grand-avg) (known)
38.67 -1.06 -0.12
40.67 -0.37 0.58
:•/;•• ^v^ปy^!^^:v^i?::i

'„ "< " ':'-"- ": "'-: :'-" --., ' V-\*!-o:
. ' ,' -/ > ^ *A- -'.' '<''"-^-; '\*'
44.67 1.02 1.96
38.00 . -1.29 -0.35
40.33 -0.48 0.46
' " , *-''>'••*'<•$*',
42.33 0.21 1.15
39.00 -0.95 0.00


Tag



\**- -
''•*, .''
"X"(ฃA
* ,


' '*
•

Data sorted by Laboratory Average
Average Tag
22.67 x
35.00
35.00
36.33
37.00
37.33
37.67
38.00
38.00
38.33
38.33
38.67
38.67
39.00
39.00
39.00
39.00
39.33
39.33
39.33
39.33
39.67
39.67
39.67
40.00
40.00
40.00
40.00
40.00
• s No data submitted
0 = Insufficient data
Lab Average Tag
NO 40.00
DZ 40.00
DD 40.00
RM 40.00
MP 40.00
A 40.33
K 40.33
VT 40.33
SR 40.67
SM 40.67
L 40.67
VC 40.67
BA 40.67
X 40.67
RZ 40.67
GE 41.00
DL 41.00
SN 41.00
QZ 41.00
Q 41.00
GQ 41.00
PM 41.00
EX 41.00
C 41.33
SC 41.33
QT 41.33
PW 41.33
LR 41.33
LF 41.33
TAG SYMBOLS
.Lab Average Tag
KX 41.33
JS 41.33
JE 41.33
DE 41.33
CP 41.33
VU 41.67
FU 41.67
AU 41.67
VG 41.67
SF 41.67
QJ 41.67
MQ 41.67
M 41.67
AF 42.00
AE 42.00
UP 42.00
TS 42.00
SZ 42.00
S 42.00
PI 42.00
NK 42.33
NJ 42.33
I 42.33
TL 42.67
ST 42.67
LT 42.67
GI 42.67
FL 42.67
FJ 42.67
tt s Above control
x s Determined to be an outlier U s Below control
Lab
EL
BO
BL
BC
AP
TQ
T
SS
J
CM
CJ
BK
AZ
UY
sx
PB
DM
CE
CA
AL
W
BN
AI
UW
UE
PV
MV
JG
DO
limit
limit

-------

EMSL-LV Performance Evaluation:
Blind-B,
18-Oct-1994
44/44 1
Cesium-137
Data sorted by Laboratory Average
Average Tag
42.67
43.00
43.00
43.00
43.00
43.00
43.00
43.00
43.00
43.33
43.33
43.33
43.67

%i
10-
0-

•esponding labs
Lab
AK
TI
SD
QP
JY
1C
HK
DG
BM
U
E
BH
TE

Average Tag
43.67
43.67
44.00
44.00
44.00
44.33
44.67
45.00
45.00
45.33
45.33
45.67
45.67

Lab
TD
NH
SI
O
HL
DT
VO
UN
MA
P
HP
CK
AW

Average Tag
46.33
46.67
46.67
47.00
47.67
48.00 ft
48.67 ft
49.33 ft
49.33 ft
51.67 x
68.67 x
74.67 x
81.33 x
81.33 x
Lab
TH
FZ
EB
CX
CQ
CS
CO
UK
QX
BG
BW
RV
MY
D
Frequency distribution
	 _. •• 	 	


-6 ' -4


1
Jl
. T ..••111
-2 T I
UlB-r
llfl.

mmm 	 m
+2 ' *

I
+6
Normalized deviation of the mean from the known value
%i
10-
0-
•esponding labs
Frequency distribution




-6 ' -4



1


1
-2 ' 6
Normalized deviation of the mean
• =
No data submitted


•.•._•_


__• _
+2 +4


I
+6
from the grand average
TAG SYMBOLS
0 s Insufficient data
x s Determined to be an outlier
ft 3 Above
U s Below
control limit
control limit

-------