United States
Environmental Protection
Agency
Office of Research and
Development
Washington, DC 2046.0
EPA/600/R-98/011A
January 1998
vvEPA
Blind-A Performance
Evaluation Study
A Statistical Evaluation
of the October 21, 1997 Data
006ECB98COV-011A
-------
Blind-A
Performance Evaluation Study
October 21, 1997
Environmental Protection Agency
National Exposure Research Laboratory
Environmental Sciences Division
Las Vegas, Nevada
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
OFFICE OF RESEARCH AND DEVELOPMENT
NATIONAL EXPOSURE RESEARCH LABORATORY
ENVIRONMENTAL SCIENCES DIVISION-LAS VEGAS
P.O. BOX 93478
LAS VEGAS, NEVADA 89193-3478
(702/798-2100)
Dear Participant,
Enclosed are the results of the Environmental Sciences Division (ESD-LV)
Performance Evaluation Study for Blind-A; October 21, 1997.
The known value for each analysis was determined by gravimetric methods,
checked by chemical analyses performed by ESD-LV's Radiochemistry Laboratory,
and compared to the participating laboratories' grand average.
The expected precision, determined by the known value, was taken from
'Table 3. Laboratory Precision: One Standard Deviation Values and Control Limits
for Various Analyses", which is based on data accumulated over the years by the
Performance Evaluation Program, and can be found in the Environmental Radioactivity
Performance Evaluation Studies Program and Radioactive Standards Distribution
Program information brochure.
Please take a few minutes to review this report and the analytical data your
laboratory submitted to us. If there are any apparent discrepancies, please notify us
immediately.
We encourage you to make use of the computer-automated data-entry system
that has been in place for some time now. As the number of participants increases,
and it becomes unrealistic for us to receive results by mail or FAX, the computer
system will be our only avenue for accepting data.
If you have any questions or comments, please send a message via the data-entry
system or contact Stephen Pia at 702/798-2102 or Patricia Honsa at 702/798-2141.
Sincerely,
/'
Stephen Pia
Team Leader
RADQA Program
Enclosure
-------
NOTICE
This material has been funded wholly by
the U.S. Environmental Protection Agency.
It has been subjected to the Agency's review,
and has been approved for publication as
an EPA document.
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997 1/30
The following pages consist of separate sections for each of the nuclides in this study with four
parts per section. After the first, each part is separated from the next by a new page or a thick
horizontal bar. The first page of each section is a statistical summary for the nuclide and starts
with a statement of the known value, the control limits, and the warning limits.
The warning limits are placed at two normalized standard deviations above and below the
known value and the control limits are three normalized standard deviations above and below
the known value. If you keep control charts, these values will be useful for anticipating problems
with the accuracy of your analytical methods.
The coin shaped pie chart at the top of the summary page shows the fate of all the samples
sent out in number and percentage terms. The pie chart starts at the top and rotates clockwise.
The first sector represents those participants who submitted analytical results within both the
warning and control limits. The next sector represents those who are in the warning region but
not out of control. The third sector represents those who are out of control, but have passed
the outlier test. The fourth sector represents those who have failed the outlier test. The last
sector represents those participants who have failed to respond properly. This is the case if no
analytical results were returned, or less than three determinations were reported, or if the results
were received too late. The reeding on the edge of the coin is spaced at one percent intervals, and
the sector shading becomes darker as the data reliability decreases. Sectors with zero width are
not shown.
The table in the center shows a number of statistical quantities calculated from the submitted
data based on the mean and median values in relation to the known value, both before and after
outlier removal. The lower pie chart uses the same construction as the upper chart and shows
the distribution of properly submitted data in terms of deviation from the known value divided
into sectors representing one, two, three, and greater than three normalized standard deviations.
The second part is an alphabetical listing, in lab-code order, of submitted data and several
calculated quantities. An entry that is shaded has been rejected because of one of the reasons
listed above or failure of the outlier test. The fifth and sixth columns are a measure of laboratory
precision. The Range analysis is a normalized value that you may use to keep precision control
charts. The eighth and ninth columns are the differences from the mean of all non-outliers and
from the known value, respectively. If this value is between 2.0 and 3.0, your analytical process
precision is in the warning zone; if it exceeds 3.0 it is out of control. A tag symbol may appear in
the last column. Each page with tags has a symbol definition summary at the bottom. If there is
no tag symbol, the data is within the control limits, but it may be in the warning zone.
The third part is a three-column listing of result average, tag symbol, and lab-code in average
order excluding those labs not responding properly. In this order, all outliers and out-of-control
results appear at the top or bottom of the list.
The last part is two bar chart displays showing frequency distributions of responding
participants. The first chart places the known value at the center and a bar at each 0.2 unit of
expected precision. The second chart places the mean of the reported measurements at the center
and a bar at each 0.2 unit of standard deviation. In both cases, a bar includes those results within
0.1 unit up to the maximum of six. Any results more than six units from the center value are
shown cumulatively by a shaded bar one past the sixth unit. If the central tendency of the known
value distribution falls away from the center, an error in accuracy is indicated. If the distribution
is broad, poor precision is indicated. The mean value distribution is similar but uses the average
and standard deviation of reported results as its basis.
-------
2/30 ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
The Range Analysis(R + SR) is calculated from the range, mean range and standard error of
the range values. The range is the difference between the maximum and minimum results for the
laboratory. The mean range is calculated by multiplying the expected precision by 1.693(for three
results). The standard error of the range is calculated by multiplying the mean range by 2.575(for
three results), subtracting the mean range from this product, and dividing the result by 3. If the
range is greater than the mean range, then the range analysis is calculated by subtracting the
mean range from the range, dividing the result by the standard error of the range and adding 1.
If the mean range is greater than or equal to the range, then the range analysis is calculated by
dividing the range by the mean range.
The normalized deviation of the mean from the grand average is calculated from the deviation
of the mean from the grand average and the standard error of the mean values. The deviation of
the mean from the grand average is calculated by subtracting the grand average from the
average of the laboratory's three results. The standard error of the mean is calculated by
dividing the expected precision by the square root of 3(the number of results). The normalized
deviation of the mean from the grand average is calculated by dividing the deviation of the mean
from the grand average by the standard error of the mean.
The normalized deviation of the mean from the known value is calculated from the deviation of
the mean from the known value and the standard error of the mean values. The deviation of the
mean from the known value is calculated by subtracting the known value from the average of the
laboratory's three results. The standard error of the mean is calculated by dividing the expected
precision by the square root of 3(the number of results). The normalized deviation of the mean
from the known value is calculated by dividing the deviation of the mean from the known value by
the standard error of the mean.
A complete explanation of the statistical calculations involved in the report may be found in
the Environmental Radioactivity Performance Evaluation Studies Program information brochure
[Draft Revision of EPA-600/4-81-004], available from Patricia Honsa, ESD-LV, 702/798-2141.
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
3/30
Gross Alpha Statistical Summary 182 Participants
The known value of this nuelide is 49.9 pCi/1 with an expected precision of 12.5; the control limits
are 28.2 to 71.6; the warning regions are 28.2 to 35.4 and 64.4 to 71.6
44(24.2 %) Failed to respond -%
4(2.2 %) Outliers '
2(1.1 %) Out of control
but not an outlier
Statistic
; 128(70.3 %) Within all limits
Respondents
~*~ 4(2.2 %) In warning zone
but within control
Non-outliers
Mean
Std. Dev.
Variance
% Coef. of Var.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
47.26
9.36
87.58
19.80
-5.30
-0.28
46.87
-6.08
-0.32
Grand Avg 47.27
7.59
57.54
16.05
-5.28
-0.35
46.87
-6.08
-0.40
6(4.3 %) More than 3 noon. S.D.
4(2.9 %) Between 2 and 3 norm. S.D.'
83(60.1 %) Within 1 norm. S.D.
of known value
45(32.6 %) Between 1 and 2 norm. S.D.
-------
4/30
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Gross Alpha
Lab
A
AE
AF
AH
AJ
AK
AL
v-> ,
^AP'V-
AR
AU
AW
AZ
->'BA;>
BB
BC
- 'nii<
;- *W* ;
BH
BK
HT '
' JMj /'
BM
BN
BO
BS
'* 'TPMDtr "
' " ]:**.W-s*
c
CA
cc"
CE
CJ
CO
CP
CS
CX
D
DB
DD
DE
DI
DO
DT
DZ
E
EB
EL
EO
Res. 1
41.6
49.2
48.3
52.1
55.6
52.7
46.2
' *, " ^?V>?*?r f -^ -tyjMfw
'" " ,V,'^' >Y,^
57.4
45.5
47.8
47.5
-:--^76jyp
35.9
52.1
;-" .', f-A?' " "i\
", '-" 'X* I., " '' 'a::-
38.4
52.0
, , ~" r* Ai
"'' '"ฐ '"' '*?*
55.5
58.8
42.4
51.8
'v--. ***," '"'"^V^''"'^ J-'i^
iv>^'>''s'Vws%:5.Cswtf * > ''r-<.'-
50.0
54.5
V-l'i- '-tv 'SA ,x.
48.6
45.0
", "*>,, /,,.-x>y\
45.4
39.3
40.1
49.3
50.0
37.1
53.8
->'-'-, , M" % -
48.0
44.7
46.3
47.0
40.0
Res. 2
46.0
50.8
48.5
56.4
48.9
51.1
48.2
*v*ซ*> *nv*^f ^.?r?nvr&"srgf
*/.!> if\ \*S^;!|;*Vi
56.4
43.8
49.3
46.6
SSii&fei^V;'
37.9
52.1
,- :^fS- ^t3r'-ป"x" *
*"' ^f^"''-f'^ \'~M
42.4
49.0
*. -'^vf*1,"^':^
58.0
64.9
41.4
50.5
J^t t "* :&"> * " <5" %" '^ & \^ >
'A'?'* ^^X**"1^^**' ^i
50.4
65.1
'xi'A$r^X<* :'
38.4
*7-9,,.
, J ^,l\-\^;^
42.9
47.4
43.7
48.0
50.1
40.2
53.9
'' ' .. - ,^
" s % ', - " '*X
47.5
47.3
45.2
43.0
V,
38.0
Res. 3
43.8
51.2
52.1
58.3
48.0
53.6
46.4
"** ,?? v s ' -^>>
S<< ~,v|#;,-
49.1
46.4
49.9
43.8
-/;7&4^
35.6
54.1
v,^ , , "^'r.v
* /- " x * *
37.9
48.0
'* '" ** """,-
%'<'' * ^ "''
59.3
69.2
43.5
52.6
i- % .x^ *-'^V""f%
S^4'""''" ""(-.V.
46.0
65.7
ssl*tr*l":':,-ll'
47.8
45.0
,"1"v- ""-'"si
39.9
47.4
50.5
48.4
50.5
39.7
54.0
, "^ !'
46.8
44.0
46.8
47.0
38.0
s No data submitted
0 =
Insufficient
data
x =
Exper.
Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
2.20
1.06
2.14
3.18
4.15
1.27
1.10
> ^ ^ ^ ^ * * '
-5' ' > , ,-
4.53
1.32
1.08
1.93
: ---oil; ,
1.25
1.15
& ; - , ]
. x \ ' ' ' '
2.47
2.08
^. "
*'\ ^ ;-s %
1.93
5.23
1.05
1.06
^V>;&-^--- " , *
%sx-^><1S.ป 0 % J
2.43
6.30
"S' - * . - i -
" " % ^
5.67
1.15
''f'"-;'~
2.75
4.68
5.28
0.67
0.26
1.66
0.10
- ?< ' " '
*'' ^
0.60
1.74
0.82
2.31
1.15
0.208
0.095
0.180
0.293
0.359
0.118
0.095
: ' "" ' "
,..,-
0.392
0.123
0.099
0.175
0.009
0.109
0.095
\ -,.,*
0.213
0.189
*'":,,
0.180
0.491
0.099
0.099
~~ -c.- '; "-t '*:
'-' * ~~'' ','
0.208
0.529
0.482
0.095
0.260
0.383
0.491
0.061
0.024
0.146
0.009
0.057
0.156
0.076
0.189
0.095
43.80
50.40
49.63
55.60
50.83
52.47
46.93
' * * ''' " ^- v \
' '"1 ' - ' '-:CtV
54.30
45.23
49.00
45.97
-"^ -^47' ; .
36.47
- 52.77
'* , """ /',-- * ~~ -.\t'
1 /" ,' Vi'V1/'
39.57
49.67
' ' . , '-' ',\% X'i, !
, 'I "'' ;'' ' ,'' '<"
57.60
64.30
42.43
51.63
^ ^ O1'^"-'^"' ' ^^ w * J V5 ^ $Q
s , <" ''' '^*% Vc,"*-^
48.80
61.77
; *'*'"- -<^;AX
44.93
45.67
-,:' ""
42.73
44.70
44.77
48.57
50.20
39.00
53.90
^ v " s ' ' '
t
47.43
45.33
46.10
45.67
38.67
TAG SYMBOLS
Determined
to be an
outlier
-0.48
0.43
0.33
1.15
0.49
0.72
-0.05
w,w, vv^wv. ^v , ^^ ^ . vvf*.
.'**f*} V" : " ฅ-
0.97
-0.28
0.24
-0.18
>-c4;OfH-;-;V
-1.50
0.76
^^ ,^ v ^-.-^-.^'^ * ^ ' "
^ "' -.^'C'"" *''"*?
-1.07
0.33
X "" l"1*' ^\ A ^ "*' * * "
s^s ^ %v>^'" ^^ ^/^
1.43
2.36
-0.67
0.60
X"4- ""^v V "'^^X-^v '''" ฃ
'^"j"^" "'I'^' % '^ ' ...
0.21
2.01
\\4i\ /." /''^
-0.32
-0.22
:>' " ;, ซ^i
-0.63
-0.36
-0.35
0.18
0.41
-1.15
0.92
;/"/ ^"r_;- \
' ,--'-', ' "1*V-
0.02
-0.27
-0.16
-0.22
-1.19
It = Above
11- = Below
-0.85
0.07
-0.04
0.79
0.13
0.36
-0.41
J.%*. V *y , ^ซ ^w> , ASSV
*$ -,;^\ - * -;
0.61
-0.65
-0.12
-0.55
r"&6ftr* xix!;K-
-1.86
0.40
"*-'\'*^-?"'-" "-**!'
?x '" '"-'M*.'' \\ ,4.*&,
-1.43
-0.03
ป-X^j',!v"'.; '!*-:-^
t\'"-' ;"'-;;*^-;-
-0.34
-0.63
-0.53
-0.59
*
-1.56
control limit
control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
5/30
Gross Alpha
Lab
Res. 1
Exper. Rng anal Normalized deviation
Res. 2 Res. 3 Sigma (R + SR) Average (grand-avg) (known) Tag
FE
56.7
45.9
' ''' t^..11
70.0
FJ 39.1
FL 44.7
;ซ
52.0
48.2
71ฃ
,- ~ x '^
42.7
36.3
72.0
1.00
0.222
0.194
0.095
;^^:p^jt;:,>r-
1.81 o!l70
0.397
54.27
46.07
^**"^'"' "" "'s* %
71.00
41.00
40.67
0.97
-0.17
29
-1.23
_36.3 41.0 4.21 0.397 40.67
^6: rv* ">1):411-* ; *
0.331
0.047
0.047
0.146
0.047
0.326
0.246
0.250
v.\, v-.\ ^ -. -, ^ v s, w
^Sd.038^
0.052
0.038
0.057
54.70
44.07
44.00
61.80
49.67
36.47
43.17
42.67^
48.37
59.43
50.60
42.73
_, ;\;C.~^i
41^73
46.80
35.33
60.67
43.23
43.80
49.33
55.33
47.60
41.13
HV^W^NX
|13i^
37.60
-1.50
-0.57
W.V Mi' ., .,
feซ^A^<
-0.64
1.69
0.46
j-0.63
iC?i^:
-0.77
-0.06
-0.81
-0.82
1.65
-0.03
-1.86
-0.93
-1.00
1.32
0.10
-0.99
PS
-1.13
-0.43
-0.85
FTiSfTO^
4*
-1.34
L- ''?S??
TK
38.87 -1.16
48.03 0.11
' "Vs"^^^*^^-^;^sw ^ ^ *".,
^,*V.^^A\, {~ -~-<: ~
-1.70
-1.53
-0.26
s No data submitted
0 = Insufficient data
TAG SYMBOLS
Determined to be an outlier
It & Above control limit
ง = Below control limit
-------
6/30
Gross Alpha
Lab Res. 1
NA
NH
N J
NK
NO
0
OB
OF
fOM
^os_
OY
P
" , t^ *\v?'*'
' m^f^'-
PB
7PD-':-
PG
PM
ฃ$
Q
QM
QP
QQ
QT
QU
QW
QX
QZ
RB
RD
;RF
RG
RI
RK
RP
RR
RU
RZ
S
sc
SD
SF
SG
SI
=
0 9
60.0
58.0
36.4
49.9
48.5
54.3
61.6
47.3
"'' ' '-'>->" /";*,''-
__45-0_
53.5
21.0
^" %x ' '^^y^^f"^ ff.
'*'f"* '*' "" *s *f'^'"/~f*, '**;-,,'*'* C
^ ^ '
44.6
-,:\'- ^ -\~''^': ^
54.7
40.3
^>%>:{:--^
54.6
30.6
50.7
46.2
47.6
37.6
39.4
58.2
51.8
38.0
41.3
7 ./.. ' ''' \ >
59.0
52.6
' ป* s V -''',""'
- - " x ," ',-"
42.0
: \" '''-:
37.4
47.9
39.3
64.6
45.0
35.9
39.3
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Res. 2
57.0
44.0
40.5
47.0
49.0
51.8
61.1
., ,53'4,
o'-1 s' *"
>ซLO^
46.2
22.8
c wp- , v ^'^tVx'V'*'?!
- ^ s -i '\^'!i "7 i
47.9
-.* Xy "** ' S % ^
59.4
36.5
<^:fi||
52.2
33.3
50.3
47.0
45.2
38.6
37.3
58.7
54.6
38.4
29.9
'-. ,-j'. Y--"-
56.0
55.1
y\ **i-\^/-\.
' ' ">--r^;-
41.0
lV/;\ - ;
36.0
53.0
43.0
54.2
56.0
41.0
38.7
Res. 3
64.0
59.0
42.3
48.7
53.1
55.6
60.2
54.3
I ^;7 <>?;-;
_47.0_
50.2
22.9
^w^w^
63.0
38.9
life:
51.3
40.0
53.0
50.4
44.6
38.0
38.4
58.4
49.6
39.7
36.6
7 "7 7*:77
55.0
56.2
ซ.' ' v-1'"^"1 "*"',''/
42.0
38.0
51.7
41.9
62.7
58.0
38.5
38.2
No data submitted
Insufficient
data
x =
Exper.
Sigma
3.51
8.39
3.02
1.46
2.52
1.93
0.71
3.81
* j ^ '
1.53
3.66
1.07
^ "^ ^ '' '.' ' " -
1.65
sx s f- ;
4.16
1.92
U^ * l^-f;^-"'
1.37
4.84
1.46
2.23
1.59
0.50
1.05
0.25
2.51
0.89
5.73
2.08
1.84
0.58
1.03
2.65
1.90
5.54
7.00
2.55
0.55
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
0.331
0.709
0.279
0.137
0.217
0.180
0.066
0.331
0.142
7' 77 "7
0.345
0.090
/ "^ v ^ v*
^ V!t
0.156
0.392
0.180
,', ' ,,'^j.'
0.128
0.444
0.128
0.198
0.142
0.047
0.099
0.024
0.236
0.080
0.539
0.189
0.170
:
0.047
0.095
0.241
0.175
0.491
0.614
0.241
0.052
60.33
53.67
39.73
48.53
50.20
53.90
60.97
51.67
f : ' *" * * ** > f S
,,,.*B.67__
7 ""' i""'-:- ~V77,'7>f v5
49.97
22.23
' "*_, W.AJV^ซWW%^ ^.*% -.^v.-.X;
f _ %" 5"" "" ^ / - / ^'^'V
46.23
,- c^, ;-HV-,---
59.03
38.57
52.50
34.63
51.33
47.87
45.80
38.07
38.37
58.43
52.00
38.70
35.93
56.67
54.63
.,,,,,, , .., ,.^,- , ;',-.,
41.67
s\..
37.13
50.87
41.40
60.50
53.00
38.47
38.73
TAG SYMBOLS
Determined
to be an
outlier
1.81
0.89
-1.04
0.18
0.41
0.92
1.90
0.61
" tr'-C' , ''
,^0.08 _\
0.37
twij:3.47^
i"^'-\''S ^ '*^%' ^ ^V" J
*'*. C v\ ,* ^'"'1 %
-0.14
-P7;;- -r^rV.-
1.63
.. :*&
\wN^'ซX ^.j^'* * f-f' >v
0.73
-1.75
0.56
0.08
-0.20
-1.27
-1.23
1.55
0.66
-1.19
-1.57
, - * ",' ':' . =
1.30
1.02
'^^'1^ : : ' :\ ^ ' ^"
- "" f ^ ^ " *7 s '
-0.78
-1.40
0.50
-0.81
1.83
0.79
-1.22
-1.18
It s Above
U s Below
1.45
0.52
-1.41
-0.19
0.04
0.55
1.53
0.24
*'".\ \ 7"'? ,*' ;,
zq.45_
0.01
-3.83 li
*. VW.-,:?V.!^..^V^^W^^A-^
% ^^v /<"""^ V ; j0 ^V^
" vl o w/"o t ^ v
-0.51
'*:- ^v tฐr:/,'
1.27
-1.57
;7;~;ivS^
0.36
-2.12
0.20
-0.28
-0.57
-1.64
-1.60
1.18
0.29
-1.55
-1.94
/*7\' v.
0.94
0.66
^,7f7^>;^4
< - ' > " ' ';ป'f>
-1.14
'7" '"7,, V, *,-7,;
-1.77
0.13
-1.18
1.47
0.43
-1.58
-1.55
control limit
control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Gross Alpha
Lab Res. 1
'-' Stfiii>
SM
SN
SO
SR
ss
sx
sz
T
TD
^TLg
TN*
;TQn
TY
U
UA
UP
SI:
VA
ฃV,ฃ^>V
47.9
42.5
43.8
47.8
49.3
49.7
38.9
42.9
_,_35^
^Xj\V\^ iS^XftJSA
, -A M* AS, *i -AVi V,Tป i.&W
50.4
__42.6^
42.2
47.9
__^^
27.9
51.5
'IIP^F
...'.'.'63.6,
Res. 2
^;i^"Hฃfv\x:<"
,v'v^ , slVS-C'^ ,,
47.8
41.0
46.7
47.9
51.5
47.7
47.6
33.6
39.6
SSSS^^.
l?A--1ixl:f^ll-.i
~45.4
^ ^_48.6
36.7
45.1
, ___4lv9
30.8
_ I5L7
;f i*-^.; -\-
49.3
Res. 3
..;v-A>.& :-.';-*
54.7
42.0
42.4
49.6
54.5
46.7
45.8
38.1
46.9
81311!?
,,^
7/30
Exper. Rng anal . Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
''> -,\ " -- -V "
3^96
0.76
2.19
1.01
2.61
1.53
4.59
4.65
5.69
C*SSX ;"""" V "V ซv*s^ซ^w^%vt^w^
c \- J o"'o''; -ฐ~ ^Vf-'cYV,^?^?!
"'4.46'
49.8 3.86
^^3<^t^,^tT:r- v-; -r;':T
* X s - \ \- v+ - - ซ \ ^ -Vs
43.0
44.9
46.5
\z. \>'' ^ ';; J -- c
44~9
40.8
s^-^f'-V'^ v "^.^v^
50.9
64.4
55.0
38.7
44.7
48.0
50.8
51.5
47.2
ซ vs., ^s ^.^^;;^^vv^>^.^sS^s
^ %ฐ " ^ X
^'X x" s *\: ^
64.5
v s o0" -% - s "
41.4
38.4
44.5
49.3
42.3
49.7
,T__
1 \ ^V-^V^Hv*
""~48.3
53.9
56.0
37.0
46.7
56.5
53.4
49.4
44.1
51.7
46.7
saraj^S wjpTun;^
--Xx-s.ป-*ซ:-fs"-\t'-
^46.5
59.7
47.0
38.6
50.6
41.5
54.7
54.1
46.6
3.43
1.68
0.26
>-'.,',' x"\',': '.,'ฐ^^?'f
2^46
0.421
0.340
0.298
0.142
?ii^
0.232
1.22 0.104
*'S?5l>1'*' ป X1-* **^ VSAWW (^^^SV^^SSV-AVA^NVS w
^7.96
-, -\ '-V-ss\\!. s,1- ''"V,.
4.85
4.53
VW.S^SVASNWSS-q.S .-. ซvs ซ%v^ V
2.21"'
5.26
4.93
0.95
3.00
7.52
1.99
2.35
1.64
0.676
^fftS
0^444
0.421
^5v>S
0.208
0.496
0.425
0.080
0.279
0.709
0.184
0.222
0.146
^l^^v '*-! ' \: T'^-- j- ' '' ' -- :
''"'{.''iS*;
66.5
;V^:'d;-'?-
45.1
38.0
41.6
49.1
,V -?" '- , ,'
59.0
^K V, ^ '.
37.9
42.6
43.6
43.2
No data submitted
Insufficient data
X
; ,'
3.88
i ^
3.60
2.55
1.48
3.47
^vo;
0.354
" ' \'
0.340
0.217
0.137
0.288
.'< ' v^^Vv;;^
50.13
41.83
44.30
48.43
51.77
48.03
44.10
38.20
40.73
^^^:งSS
45.77
^47-20^^
40.63
45.97
|^^^F-^j;
28,20
50.90
- r "i^^f^^^y
~\ ปป >\ * * "- * -f C-~ ;~
. /' Tj??:4!." ~".
! , oCl'-M^V,^^"" ; -~s, "*^
-*t-~iif'7"!-!'; % *%-<,"
~.y;\;- -, ,-- ,- \5>:,-
46.30
,_45jH
TC^' 7 T\;5X'KT J^f' 2"
48.67""*"""
59.33
52.67
38.10
47.33
48.67
52.97
51.67
46.97 __
' >ป .-,.! 1 ,, %
:; ^ !S-;^i
63.33
v><,--^.c^,;^
41^47
39.67
43.23
47.20
TAG SYMBOLS
= Determined
to be an
outlier
^i^4^^
0^40
-0.75
-0.41
0.16
0.62
0.11
-0.44
-1.26
-0.91
*XV *%'SA^^S8^*T^!N*w*v%
^ilS-3
-0.21
.^04^stM>
-0.92
-0.18
^2?64
0.50
^^t ^T fTT^T^,
llrSV^L
m^r"'Tx7-7v;;
,- /^r^
';!;^!x;^N-v-1\,i-!
-a 13
J0.21 ,
^-IJKl^V^^S^
0.18
1.67
0.75
-1.27
0.01
0.19
0.79
0.61
_-ai8
\;V;,;;, !!
:VJVXฎ^
2.23
^3'*v^v;\
-0.80
-1.05
-0.56
-0.01
ft s Above
& s Below
^,^S^-i ,ซ-!^
0.03
-1.12
-0.78
-0.20
0.26
-0.26
-0.80
-1.62
JL27^w _
r'ck, ."0. !!\J^;K.^-"V^
-0.57
;9A?,^S ,^
-1.28
-0.55
"-3.0l" "*~V
0.14
^_^^^
jyS,^I_
V T* I'^f-x'f**^
-0.50
-0.58
fpfiv^i^
-6.18 >s"" "
1.31
0.38
-1.64
-0.36
-0.17
0.42
0.24
-0.55
*S5 -.^o^X""* *" * s*"sA<"$"N
%r\\ ^\^'9^i.
X*'.*- .!' >.% ^ "^ s ,.\ ^ V* * .X1- -\; *
* s^ % " wS^^ V*^>X *^ *
1.86
^%. ~;^;^
-------
8/30 ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Gross Alpha
Lab Res. 1 Res. 2
XN 34.4 33.4
Exper. Rng anal
Res. 3 Sigma (R + SR)
37.2 1.97 0.180
$ '' i * "' '
-,.'. * '.
* V* - -;": ,:- " ' ,'' '' , , X "'"
Normalized deviation
Average (grand-avg) (known)
; 35.00, __;1-70, _ _^-2.06_
Tag
^r$
Data sorted by Laboratory Average
Average Tag
13.77 x
14.33 x
22.23 1).
28.20 U
34.63
35.00
35.33
35.93
36.47
36.47
37.13
37.60
38.07
38.10
38.20
38.37
38.47
38.57
38.67
38.70
38.73
38.87
39.00
39.57
39.67
39.73
40.63
40.67
40.73
41.00
41.13
41.40
41.47
41.67
41.73
41.83
42.43
42.67
42.73
42.73
= No data submitted
0 s Insufficient data
Lab
M
FN
P
UP
QM
XN
KT
RD
I
BB
RZ
MF
QU
WE
T
QW
SG
PM
EO
RB
SI
MV
DD
BH
XK
NJ
TY
FL
TD
FJ
LT
SC
XJ
RR
JY
SN
BO
JE
JS
CP
Average Tag
43.17
43.23
43.23
43.80
43.80
44.00
44.07
44.10
44.30
44.70
44.77
44.93
45.23
45.33
45.67
45.67
45.73
45.77
45.80
45.97
45.97
45.97
46.07
46.10
46.23
46.30
46.67
46.80
46.80
46.93
47.00
47.20
47.33
47.43
47.60
47.87
48.03
48.03
48.37
48.43
TAG SYMBOLS
Lab
ID
XL
L
A
LE
HI
GZ
SZ
SO
CS
CX
CE
AU
DZ
EB
CJ
VJ
TN
QT
X
AZ
U
EV
E
PB
VI
OS
UA
K
AL
TQ
XM
WH
DT
LR
QQ
sx
MY
JM
SR
Average Tag
48.53
48.57
48.57
48.67
48.80
49.00
49.33
49.63
49.67
49.67
49.97
50.13
50.20
50.20
50.40
50.60
50.83
50.87
50.90
51.33
51.63
51.67
51.67
51.77
52.00
52.47
52.50
52.67
52.77
52.97
53.00
53.67
53.90
53.90
54.27
54.30
54.63
54.70
55.33
55.60
IT = Above control
x = Determined to be an outlier $ = Below control
Lab
NK
VO
D
WO
C
AW
LF
AF
HL
BK
OY
SM
NO
DB
AE
JQ
AJ
S
UQ
QP
BS
WW
OF
ss
QZ
AK
Q
w
BC
WR
SF
NH
O
DE
ER
AR
RI
GQ
LL
AH
limit
limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
9/30
Gross Alpha
Average
Tag
Data sorted by Laboratory Average
Lab Average Tag Lab | Average
Tag
Lab
56.67
67.60
58.43
58.47
59.03
59.33
RG
BM
QX
VA
PG
VT
59.43
60.33
60.50
60.67
60.97
61.77
JN
NA
SD
KX
OB
CA
61.80
63.33
64.30
71.00
76.47
83.13
x
x
HK
XF
BN
FE
BA
KE
% responding labs
Frequency distribution
% responding labs
-4 -2 0 +2+4
Normalized deviation of the mean from the known value
Frequency distribution
10-
-6
-4-20+2 +4
Normalized deviation of the mean from the grand average
s No data submitted
0 = Insufficient data
TAG SYMBOLS
Determined to be an outlier
1t = Above control limit
U = Below control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
10/30
Radium-226
Statistical Summary 182 Participants
The known value of this nuclide is 5.0 pCi/l with an expected precision of 0.8; the control limits
are 3.6 to 6.4; the warning regions are 3.6 to 4.1 and 5.9 to 6.4
89(48.9 %) Failed to respond
9(4.9 %) Outliers
5(2.7 %) Out of control
but not an outlier
Statistic
. 71 (39.0 %) Within all limits
Respondents
- 8(4.4 %) In warning zone
but within control
Non-outliers
Mean
Std. Dev.
Variance
% Coef. of Var.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
7.15
15.88
252.24
221.98
43.10
0.14
5.00
0.00
0.00
Grand Avg 5.05
0.70
0.49
13.90
1.08
0.08
4.98
-0.33
-0.02
14(15.1 %) More than 3 norm. S.D. ,
8(8.6 %) Between 2 and 3 norm. S.D
,47(50.5 %) Within 1 norm. S.D.
of known value
Between 1 and 2 norm. S.D.
-------
11/30
ESD-LV Performance Evaluation: Blind-A,
Radium-226
Lab
A
AE
AF
AH
AJ
AK
AL
< A*"k^"S*
" ?*MVA
"'-An','?
'ku'r
AW
AZ
BA
BB
BC ^
rปBOif
BH
BK
/BL";
BM
BN
BO
'IBS:;
B^
c
CA
xGC--
CE
CJ
CO
CP
cs
^iXW
ex.
D
DB
DD
DE
DI
DO
DT
DZ
E
EB
EL
EO
=
0 a
Res. 1
4.7
4.4
5.1
4.3
5.6
5.9
5.6_
ฃ,^ jv.^ ^^f^s?*"*^
'- "*'"* -fi'*,^ ,'//-'
;v'7?;;^iy
iV' '**&*: ;-
4.6
6.5
4.6
4.8
4.9
;>iSV ^'Hf;'^
5.3
4.8
;'**<*?*,* XV' ;',
5.1
3.5
4.7
^ ' X- "v ;-'
"' : >', ^''""/
5.6
4.5 _
^, ,,^ ^ ^^
5.1
6.0
5 T ";,v; '^
. '> "- - , '
\ ',
5 ' * *
',, ,,>?. ,',,,,, , 'V
5.2
- - v, .:, r.
5.4
! '"' ,,.' . ' <'
4.6
4.8
4.9
4.0
5.3
4.8
Res. 2 Res. 3
4.6
4:6
4.5
4.0
5.9
5.1
4.9
i^ * *>* ^r^^/x^ '^r*^/, ^i^< T^.V
:f *'f'f-2:J. :-rf ^-f --? -'? '"
T|^% ^$^':^f
^llyivKi;'^
4.7
5.7
5.4
5.4
,, ~. 4'9 ~
<^r^;V^^K'
4.3
4.9
JlV'^gfL' \;:
5.0
4.1
4.9
.- .-.... <- ^ ..'...!..
1 v; tf-}"- 1\ '-
5.1
4.3
; 7'-^ <3-? ' *?",'>
4.3
5.9
-',";>"-" "'","-<; ""' '-",-
" \' ' "-. , \_ - -!'
,'>" ' !--' '-" * >,~ ' *
'-, ; ' ,'-' "",';" - ";
s J'' * *
/-- K^"."^fA'"-
; ,--;,'- ', i's , ,,;
5.3 '_' J
'.-.-V-1;" ,s;,':-f' -
5.6
' , '' " ' v -"- , '
, / ' . '- ..; '
4.0
5.9
4.8
4.0
5.8
5.0
4.7
4.7
4.8
4.1
5.0
6.9
5.0
w ^s ^ V^.^^...
;Ax v ^ ,:
%* '''. *'* v
'^rt rt'' /^
5.0
5.5
4.5
5.1
5.1
- ;"<-,; \x"x*
4.2
4.8
x ''"'' T ^ ^\
5.2
4.1
5.0
'*<? s '^
' ""' ';"'' /"*
5.5
4.6
Ss'.v ' *
5.0
ฃ.8_
*'- -.
s \ "" s'-
v\ .. ' -"
4.9
5.8
' ; - -^
4.7
5.4
5.3
4.1
5.3
5.7
No data submitted
Insufficient
data
x =
Exper.
Sigma
0.06
0.15
0.30
0.15
0.46
0.90
0.38
"^^%^VV ,x*
'-''v" ", V
h-?'; ' r '
'*ฃ"%$}& '""
0.21
0.53
0.49
0.30
0.12
v:V, '-V'X
0.61
0.06
.v'" " -, ',,,,.'.,,>,->;
0.10
0.35
0.15
0.26
0.15
'- s
0.44
0.10
s
,' -'
0.21
0.20
-ป
; -;'"',
0.38
0.55
0.26
0.06
0.29
0.47
Rnganal
21-Oct-1997
}
Normalized deviation
(R + SR) Average
0.074
0.222
0.443
0.222
0.665
1.627
0.517
. , wv ^ ' " f j1 ^ ^ x -.' fl'Tf ^ffy
. ^ , , ~"'-\'^~ f;. '^V'"
-\^-: >X"VO-'^
% ' Otl4rf\f;f;*??
0.295
0.738
0.665
0.443
0.148
' *,': "".' '"',* ,V'
0.812
0.074
:, ;-/:?;;^*if^
0.148
0.443
0.222
0.369
0.222
- - x ' r
0.591
0.148
"" "' ';;'
" '
0.295
0.295
0.517
0.812
0.369
0.074
0.369
0.665
4.67
4.57
4.80
4.13
5.50
5.97
5.17
l^""*" vX' ' - S?-
SIM";:^>. }/
5^|S^^:'^i
-0.62
1.83
-0.48
0.10
-0.19
^V^^J^" ^
-0.98
-0.48
|ST7-L^
0.10
-2.50
_^_-0.41__
'"-Vป-~ ,; -,,;ซ" v
'l,"!^- -," ~s '> ! ;'/
0.75
:1.27
w ซ:-. ' ^ >' " % V
-0.55
1.83
tpr-^-rj^
-//- " v - " "" *'f
> * > ^ ^
V \ ''"' /;
'' -.:' "-"'"--
'_,'"0.17
,*-- :- -' ^
1.18
""'^ ~ ' --,
' ,./-,<- -''-'- - ' ->.
-1.34
0.68
-0.12
-2.21
0.89
0.24
tl = Above
!! s Below
-0.72
-0.94
-0.43
-1.88
1.08
2.09
0.36
Xw^Sf,? ?x?s^;gAS''^fV^7^J;'-
IV, ""-> !=,;" ,'*;.~^
^^':lfe''i*B;
J-SSl^^rxS
-0.51
1.95
-0.36
0.22
-0.07
^Vf'f f -#-!?
-0.87
-0.36
^A5ฃ,:!;^i>
0.22
-2.38
-0.29
o?^'\ *"'>" ->*',,
"-^r'-vJ''"'*; :
0.87
_;L15w __
" A',-^"^'V jป V"
-0.43
Jl.95^ ,^,
"""-""^"V^"''-
,/: - -!- x , : - >, ,'
"Vs" ''/- ' ป' X''N
j , j ^,
V ^ < ^
-';' '-'':'": '": *-;' :
C\ OQ
> :--<"-<' -.,;/-
1.30
"'".''^^
V "' ;^;-:i*>:^
-1.23
0.79
0.00
-2.09
1.01
0.36
control limit
control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
12/30
Radium-226
Lab Res. 1 Res. 2
Exper. Rng anal Normalized deviation
Res. 3 Sigma (R + SR) Average (grand-avg) (known) Tag
ER
4.9
5.0
0.06 0.074
4.97
-0.19
-0.07
FN
G^
GQ
5.3
53
^
3.8
5.0
! Y
2.2
0.17 0.222
-^?*^'Y"
1.60 3.596
5.20
/^|
3.80
0.32
-2.71
0.43
gr^n
' C v'
-2.60
HK 5.0 5.2 5.1 0.10 0.148
HL 4.6 5.7 3.6 1.05 2.049
5.10
4.63
0.10
-0.91
0.22
-0.79
I
ID
5.0 4.9 5.0 0.06 0.074
3.1 3.5 2.5 0.50 0.738
4.97
3.03
-0.19
-4.37
-0.07
-4.26
JQ
JS
JX
JY
K
5.9
5.3
6.4
4.9
5.5
5.2
6.9
4.5
5.5
4.8
7.7
4.8
0.23 0.295
0.26 0.369
0.66 0.960
0.21
5.63
5.10
7.00
1.25
0.10
4.21
-0.69
1.37
0.22
4.33 fl
LL
LR
LT
M
6.7
4.5
se;o
6.5
4.4
16.0
6.1
4.4
12,50 31.441;
0.31 0.443
0.06 0.074
6.43
4.43
2.99
-1.34
3.10 It
-1.23
= No data submitted
0 s Insufficient data
TAG SYMBOLS
x = Determined to be an outlier
tl s Above control limit
= Below control limit
-------
13/30
Radium-226
Lab Res. 1
IMA
, "v ,,"' ',<,,>,
ESD-LV Performance Evaluation: Blind- A, 21-Oct-1997
Res. 2
"* tfl^^jf -;K >,
Res. 3
>;/!" 'v %
Exper. Rng anal
Sigma (R + SR) Average
',;-
V ',. - "--
)
Normalized deviation
(grand-avg) (known) Tag
'-' .._> ' -',v?;, -' "-V-
^ , ซ-"-ป4, < ', ', '
-'WA-"^/*^^/.'-, ,*ป xi'Vซis<>'' .i"^;"?*^ 7ซg^>"?iwx ^'/A ..',><;-,', *'&'*'" -f'^\' -A" ' "'- -sv y;,-";'^^^-','1^-"'"^1-^ >..>'; $*?'& *'&. ~F-.y* ; " ^sw^v^s <,-**-
NH
NJ
' j||t' r
NO
O
, OB
OF
s^^ซ*'''
' C IRff '
, ''' ' V i ,-'
:-;,08rฃ
<>OXi
OY
p
* X %
*7*iป%\'
PB
: i"D''.r
PG
";'PMฃ
PQ
V ^W' >
'&#*
Q
QM
-""tol-fr -'
' f^T s
QQ
QT
;.QE,
> & &$ jfi '*?', 3 <*
' !> , Vv, * <<.*/"ฃ,
:/''> ; % " '^ ' '-ฃ* "
^/V-i-'?''-;
4.4
4.7
ftV-L " J' ,', ' % ^
' ^ ","ซ. ^
5.1
>' C ,ป*>>"'
3.5
<;;;~^ !,<
~ , T'-'"" '- $?*
"' = ,^%' '*" ; " '
;- ,^:, 7,4>';'"->
7.6
4.8
-" v^ -.-"' " X ^ -. ^
^ ^ ^^v * ' '*
6.2
5.0
5.1
-" /' -',\;' '' VT
r* r/^c
_V.7'
o \ ," ,""s V ^
!?'J;ioi^
-'-, ':- ' ,. <;'
? j '' f ^
" *-
5.3
. ' '-. ". ' u ' >
, y^ ^ < ",;
' ^ w'-'* ^s' ,x
1.9
5.1
4.4
8.7
4.9
4.4
4.6
5.8
rr^q^^,.!^
5.5
5.0
-' X^, '"/,-,
4.4
>-.'^V ' ^ fJ ';vv
'^v''' / ^'-i',t~,' y\f*"^$~
HT>S$ฃฃ*2&
'7-**^?^
4.8
5.4
.%Cft % ^ M ^ V.
%"*'''', ^X\'*'
5.0
'" /r;?-?--''
3.9
^-j'^^W-
,"" ^vi vr^-
* **'ป*''':' ^^ '*%*
-'= -'-\?ป8'^;
7.1
. ,4,-8_
^ s Vv, \ ^"*v-sซ
-^ ' v-- s S^^V^- *.;' J
5.9
5.9
5.3
I- vV"" \vJ";
f:^งC
4.6
;.;'- -"^-S; ^~lv' "
rliife
' ' '-" ' , -
' ' "^'cf'^y?
'"' ',-<"'/- ,
5.1
, x **.\f X V" ^^
,".V;V, J*"5.\,
< ^ A ' -. v
/IS-'
4.8
3.9
to
5.1
4.4
5.5
6.0
g~^ .^ ^
5.6
4.7
v,v%,^ - - . ,,-.
3.6
~ * " A ~ ' ^
/>'J ^ '' S
'-, >,"' ' ^
j';V\-". , ,;
:/,-='-/ --'-
4.0
5.9
% V. ft tt
5.2
V^/' 0 "v - "
4.8
ti'-^"" - ;-
s-x ;' ^,; Vt
' . s " 4 Ov ' *" s
^" ' .- - -7ซ8 ~-;
7.0
4.7
A* ^V ' " "" \^ !-
^ ^ '""*,. ^ '
5.4
5.6
5.8
v>-'/'~ rV^*
't?^;;
,, 4;1
;,,"""->! ,-
'uVjiii
, ;\1 - , '/ /
,f!:'K..3jt?
sJ:." -^%:\
4.8
^^, ^ * J s^ ^ ^ ,
'-'" '''* ' ' "'
*;"l', ", - ,* ,..
/S % %
2.0
4.8
4.9
7;2
4.7
^
3.9
s No data submitted
0 3
Insufficient
data
x =
0.52
0.47
"; ;' ' -- : '-
0.10
0.25
. -/
0.46
' '
-,'' . ;.
-':V> '' - ,'-
0.40
0.60
0.10
0.67
I ,-;' -;~-
J ^ " f "
A ; ,' "" '
' Vป%\0ป2I>v- -
0.32
0.06
** " ' ' '* * f- 0*^'-
" ' - " "' i! -- _,' ^ s ' '
0.40
0.46
0.36
, >f~V ," - "- - ', -
ฃi;?2^i":^:
0.15
;'.; &4Q '
0.25
' - ,
0.10
0.17
0.50
0.93
0.20
0.29
0.665
0.665
,' -,'',",-
0.148
0.369
- -'<':,-<.- '"
0.591
's ' * ^ S " \ ^ ""
J ' \ '', ^-
,; \ '"'-I } ,< **
'' , ^ /''' ;;'\,' v,.;
* - ".;'' /'v- "" ' .
0.591
0.886
V S ^ .
11 *
0.148
,- - - - -
0.960
"' ",:- '-',- !>'
" . , - '-A;X".N
' '' /: > '* 'ฃ . x
0.443
0.074
**f ,"" ^ " ^ Xx " -
ป x -
0.591
0.665
0.517
"v" "' -' ^'"^'"vC
5,846- II^!
0.222
-'" V-!'-"'%-
0.591 =
- 5
0.369
C " ' * X '
0.148
0.222
0.738
1.486
0.295
0.369
4.90
J3.17_
T5 ^^'"c^y
5.50
4-,7?.,.ซ
\ /-i, "-
4.13
1 X (* s >A^
'-. ^'i:.1-
ss s V'\ ' ^
-cV-k >vV^
""x."' i
4.40
5.33
^ s +*ซ.ซ '
$s>r
5.10
!-V--< \:--ซ
4.07
^:l>>>
-"\-r;^{7
^^^ , V*^ s
:;7t67^:'
7.23
4.77
Ih}.^ V. .^.AV^AV.
^V\'x"o*''^
5.83
5.50
5.40
T- f , 7",
16160
4.57
' ', /<
10.27
< '
5.07
< ; " ' * -
1.90
4.90
4.40
7.63
4.90
4.23
TAG SYMBOLS
Determined to
be an outlier
-0.33
_2.41
- ; ^,--- ->,->- " -^x1'"
0.97
-0.69
'V-,';*' , .ซ; V% ~'-l%
-1.99
^ ^"Jl- "^ N v< ^ ซJ^ >^'"t^
%^'*'^\ . ^^A^''
*%> ' ijX'-v/'1' -".ซ,'
AV^^'l^vV^
',>- ' ;-y '/"- ,' -
-1.42
0.60
% ty.v ^ S s S s Sf sS
, * * s ' i -. s
; '"" " \" "f ^ ."
0.10
--*' " >:f^"vv''-
_:2.u _
/\:0V\,^s^^s '-
V 's ^ s ^ " ^ ^ ' ^
^ ' '^^tt1^ J " X"
4.72
s_^.62
\; Jjjj$jf% $*^ - '_ >ป^?^J
^ v ^ ^ ^-- '< ^ ._' * " ', ^ s-.* '>. __ ^
1.69
0.97
0.75
' Y"~" \, H~^~^v"^ ,'
iViiodfex
/v's -1.06w \"
,4,V'" ' ' 'v ,,- -
HMta&T?!'
-\- ',; - ,",';- Vs
"** v" ''*?''
'' ^
0.03
~'sy,--A'^'' '"-"
-' ,,v ' , "' >
V, >w'Vr; Vy
-6.S3
-0.33
-1.42
5^58
-0.33
-1.78
ft = Above
U s Below
-0.22
2.53
's"":H|'^?^y<7
1.08
70.58
-' > ^.^"-'J^m^
-1.88
-- - \* ^-^ ' - --' ' - ~5
^ ' * 'A N - ' &' * ^
U/1-' ' -i!\ป - -, -' >''
p,,,';;;.C^f', ;ซ/ %-
v.^-i^-vv;-
-1.30
0.72
A \ s ^ * A% j wt v; s " v.
A s^ ^Y/^ > V '? '-^ % ^
0.22
' ''- :,"' ;<-* ';:'":
-2.02
;:\^!F'!*n
;,;''' '^* : "'iV''
* 5 . ;-% **"^>*fev%^:t
--^iSB^'^IX^ '
4.84 tt
w-O.J51%%%
^ ^-"l- '""-'''' ," ^ ^^-"^^
""' "" ^ \ -1'1' - Jjt -
1.80
1.08
0.87
"Tr^--*^'^ " ' ""'
ie&^'S". 1
%^>.94/",',l
- '";'""'' , ''"*"C-i
iiJof^t^
'!,;--- '=-">- -- ซ-;V*
r/; >";' ?:'
'-,' 'v'-''-",,* "v'
0.14
**''" %' f^'\?v;'/ f x^c ->v sx*>
;% ^ .. ^ ""^^j'* ' y ^.. 0 ?' -'
^7','j'U".,*'^,
'; ' - ';<, 's ''>;:
-.6;7i;<-,;, x
-0.22
-1.30
5.^6 x
-0.22
1
-1.66
control limit
control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Radium-226
Lab Res. 1 Res. 2 Res. 3
*SM
' 'fiitf~*-
'2r
ss
SX
sz
T
TD
- 'ปWtf 'V
"TJU V
TN
TQ
',' sV
Vnriy^
ss s A *' ,
u
ruA?
uK-ซ
UP
ฅ9
UY-';
VA
''VCT
~ -- -X
s,'V,Hu
^vT'
yy^sf-
VTWf-
- Y$V
s%^*%
.'tyf '
w"
'' -rtrrr.
WH
WO
'WR1
; \^ ^
- 'iBUTfltf
;W W
x ^
.XXAl
*-JL&'*
:^ko!
!!~rrU-s<
\3JjJT
'''- ' ;^
xj
, XK
XL
XM
ox""" ^v ^ ox^,A* ^ X" ^y'"
* , " - * ' ฐ S ' , ^\ A ^ , ^ X-.
vsXX,^-' ^-'\'" "s, ;
^filtl
5.1
5.1
5.1
5.1
3.7
> - ;?> -~,;-^;-,j;\"- V-^-j^',-1'*";5;
- ,-s ;, ,.X ^ . ,V^'"~ - _
5.6
5.0 _
',A--/ -^-H1-"^^
N?\>\S' \vฐv ^vs' ^ CA <-s
^^ ^ ^ ^ s Vv Vl ^W V'^%
5.2
sr\:^&55y^:
|~ > '"-Cv-i!" '- "' ป>^i-^N'ป
5.6
4.9 _
;\: , ,,,;"V ' -";'v
"'e'.i"*''
1 , "1\ - ;,-'\\v'\ 5
>\,\ ' -, , '\:V\\ v .
' , ' ' -i.xf "- -
/.r ",5;8,,"
s --V?- ' \ ^ - -" -!' -;-',- -- ^
"-'s,;s' ^"f~r~"' ^,""~~'-'
' , ^\\Vv ' ^ 'X ^^v' v ,
5^\*v^t<^ s-^\x-t sv ^
:\;:^|^^Y^
- ,..^> -,^>^
s^ _.^ , ซซ. , : \; : f ^ . " '
4.9
3.2
T\Cf'~.;^^|tH *
-,- v\ X'" ^ ^""o .i-.x S-ปl^ -.X. ^ * ^
%5 " %Xv ; ^ ^ ^ C^" ^ ^V Xซ*v\- 1 5 %\*I ^ ^
T * *0 vsiss' st^S * " ^JX^'^\
1^J_A8^L^_
|"^||^5^7^
f/^X' s;\ ^ '^"i-'^-v
r \~!^; -;0' "-*~v ;Xs :
\ ^x T ' ' ' ' * 3 I ' **ฃป*
>V !1 V ,' v> x; - 'ฃVc s '*\~>
u?". -!^V".~"ฐ^Xซ <,'"-"'"
\;* ' %1 I,*1- - o !s V
- '* " ~\;" '' " >\
4.8
4.5
5^3
-/;>;\ , -
!\:^V-\
4.7
5.0
7.9
5.0
4.0
,~ SJ^-'^^TX jh
N><,- - . , "
5.3
,4:9,, ...
s s** " ^ \v<"^^ l
* % ' " " " / \
x% s " \ >v
5.3
-f'S-1-
* > \~ ^ s "-
5.7
4.9^ _
" " s ^ "" s -.
6.0
ป" %;V:^
> ,!\-VV ~
,5-3.,, ".
' sV,v^'^"-;x
,,';\\, "' '"
^"-\\s^ ^ J^
V ^O ,5
J^ISS-^
*ฃ-'>
^(r':\~;x ^
4.7
4.9
rr"!'^^ :
^ 1 x ^; s-^v^ซ.v -.^
^ s^V^^'x'"^'.'''*^'1'-1-,
' " "-." " -.^x""^"
^5.0
?T^jc
,r": 5 , - *s " s
\,,\ i;^C <\-
s' -xr,~v - -
\ x^^-- \1^ s^ ^
'?^f :,
^ ^ ''"','
x, ป^vX -
5.0
4..2
5.6
* ^ * -.x
5.0
5.0
6.1
5.1
4.0
5.7
4.5
. . '-' -
^ o x V
* X^ S ^
5.3
<-djfii:;:
6.2
5.2
6.9
^
' > -
^
5.9
" \X ^ ^
^-**A ? ^x1-11* \v
4.9
T'ฐ'!; o'" ~ '' -
4.7
4.2
s" *
- "-^ "x" "" -^^
" "-X \
5.1
r^ ''--"
~fe";'v; --:~
V ^ฐ ^%^ " ^
' VC'": " s
; \ v" " "' "
5.2
6.1
= No data submitted
0 e
Insufficient data
X =
Exper.
Sigma
0.17
\ s v
0.21
0.06
1.42
0.06
0.17
s o > ซ * ซ x
0.21
0.26
0.06
'";VA26\
1 l ฐ x %
0.32
0.17
0.52
^ s "
0.32
/- ;\X --"
0.15
{7 i;<---~ % \l
0.12
0.85
0.15
N "
- X v- '
^ - ,
0.20
1.02
14/30
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known) Tag
s -Tx
0.222
,\ V -vv -
"4;!^
0.295
0.074
3.033
0.074
0.222
.
0.295
0.369
^\\ "
*"\ ^^ ^ V
V , . ^. ^ ^ ..
0.074
Ol36ป
, >
0.443
0.222
>N A % '"*
0.665
,-s
0.443
\
*-.x V -s*1
11 "" ^t-x ^ ^--x^^
s ! ; ฐ t -' ^ "
0.222
', o\^ ^ ":\"
0^148
1.486
0.222
\ " % .' '"- ' s^
X X ^"^ * oXv x
" s , ', "
!' >-.'
0.295
1.767
5.40
V S^" ^ ^""
!. /.'^:i'.."rt
4.93
5.03
6.37
5.07
3.90
-t v->^ * xv^' r " \ "' '
'''.-\"~ - -" ^l-i"-f
5.53
4.80^ ^
%-s'.'vV^x(-^"/'
'' ' A'"^ฐ"^x''X^VsV^
^ ^ V " *V?X >
5.27
^?3ซ,;:
, >-^\- \1K'*X" ^,~' v\~~ -
5.83
, ,._.J5-9S_.
, ^v"x ^X1" \ \\x*
6.60
-* v!x~V o,'\;'*
'* -;-v;sV*vC^ ?'
"^ '! v^" ~;S* - '
"e.67_ '
~\X- ''-: ' - ~i"-0l^
= .. v ^- \*0.
--- - %'ซ-^*;,*
""----- ' , N - ---^- ^-
v;^d"^^^?
4.77
~,r-~ " ~ "rr ~tv!---
4.77
_4.10_
r ^TT^,\ .'>3SF
x "v^ X;\^ V^^^i -"^ AXV ||C- ^^%
^X "* '5-.^^ s" ^ ^"^ \X
"" v '"- *";** , ' "? -"--"
4.9_7_
- AU ,$V;,cv't^%
- ^ -" ' s- VX --V ^\v"'N
/:>v ?'--"-" "^ ;--x ^fti
"-4.,N;-T,,-; ,- ~^-;>|!^;\-
-'*-,-! -~- \ ---* 5
-;-;r:v ---^-;r>^
- -v; ;;!;, ,,s 'j-'V-
-x ^ - - x^, -
5.00
4.93
TAG SYMBOLS
Determined
to be an
outlier
0.75
' ,"- \^V 5\\ \"'.
i||||!
-0.26
-0.04
2.84
0.03
-2.50
ปw.-y,--ป<--v-,~\ ~^pป>
^ "" *" "" i J^'^
1.04
^v-0.55 _m>
^''-P^-y'H-Sif-
' * -V ^- I- v ' v ^-A;
' Xs ^ ^ - - - ^^v%<
0.46
^^
^ ฐ^ " s ^S^X "s*
x"^x"N v U; vxo^"^"" * x
1.69
-0.12
-\"-\. ' ~ , -\ j\N~lXr
3.35
\'~\- !*S-' ,.N;'
A,- "v \-\V\- ,X '" --
v v ^ '""X^^x o s '""
1.33
.V,'X~ x-v-~t **it'-- - '*
4\i^ฐx".;\r.x'
SxS\ V xivx ,-,, - ' \- ,--
vV^'tviv *' vr-'ฐ ,,ox
0.87
,\~ *i i\'
0.58
^!*1S
-^-Av\x-x Sf1 ;\<|MK><\ x
1.80
0.00
'' s' '.V -\'f'V;- .'
3^46 tt
* ฐ , - ' ,! -xi -
-V^k;\--/x;T:S\
- , v*x.-\-~- - ,**v
1.44
\\".,x-"" kt
-X.VV* \ * ^ "v * * A*>% *x'
X$x.^ ? ^- >%V--'- ^^:T ^
-0.62
^;W*---?X-- V-X-X -
-0.62
_:HL ,
^^;,^TT.~v
v^^x''-;.^ ^^'i'l v "^J^vs
11 "" Xi^*1'^ % >'"'" ""vvVx-V
- , <" -. ir " v -x ^ *\v xv x^-"
^^-0.19vvv
*-\iiil^%?4^^ ? ' ^
\iv";r;" \"& ^V-
^.^ r^V-^;
^ tl t-5"w;I ~ ^ * -s- '
\v-t-5?'' '^ - ~ s
f tT1- '-'-' '-'' ' ' "
^\,, V- -' 1 - '
\ ^^ '- ' ^v - "
\ -
-0.12
-0.26
tt = Above
11 = Below
-0.51
s- ^s-j> - ซ-^py-~~.^
-0.51
_:1.95____
F' ,% "^"JTfS^I?
0- ss " * '-""xt-" ^Vt| s\^V SJw 0
""J ^ > ^XX^J,;'1' CC^\ ^X.^i1'
0 "s^i S^ *^*ป^;
,;0ฃ7_ r
Al^V^-^^.
- s^! ^.* Y^tv.'Hs
^\tx^^Q^^II
;.Xs~^ - x'ป X-;Xt{"~3|^ x{^
^ ^* V '" ^.: 4-*- ^ f*
'!\*r ^~:X--'^-?-
V- ^V:^*ฃ
"ซ ' >Vฐ' vป - '
h~ > -, , ,^ ,, ,
0.00
-0.14
control limit
control limit
-------
15/30 ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Radium-226
Exper. Rng anal
Lab Res. 1 Res. 2 Res. 3 Sigma (R + SR)
; 3BN^|r ; ^k -,; ' :=-<-- -,' ' -~ s\? "<-:,^-p - "
- ' - ' " < *,;*."' -' - , . ' '" - '
Normalized deviation
Average (grand-avg) (known)
'' -: '
.'-^""ff > ^ '"''''" ^ ^ "^i. *N%sxt*X'"i-s v.1" * ' V'^1-
Tag
i . '" .
:^o^;:: -;;: }:^;>?frtv^i>v' ; -" *: '-'"/ , ; * , ""xVr"' f -Hr/.'^t^^i;^
Data sorted by Laboratory Average
Average Tag Lab
1.90 x RZ
2.33 x AU
3.03 li ID
3.80 GQ
3.90 TD
3.90 BN
4.03 EB
4.07 PG
4.10 WO
4.13 OF
4.13 AH
4.23 SI
4.40 SC
4.40 OY
4.43 M
4.43 L
4.43 DT
4.47 CA
4.57 QZ
4.57 AE
4.60 BH
4.63 HL
4.67 A
4.73 O
4.73 K
4.77 WH
4.77 W
4.77 QM
4.77 AW
4.80 TQ
4.80 CE
Average Tag
4.80
4.83
4.83
4.87
4.90
4.90
4.90
4.93
4.93
4.97
4.97
4.97
4.97
5.00
5.00
5.00
5.03
5.07
5.07
5.10
5.10
5.10
5.10
5.10
5.13
5.17
5.17
5.20
5.27
5.33
5.37
Lab
AF
BK
BA
BO
SF
S
NH
XM
ss
X
I
ER
BC
XL
UQ
E
SX
T
RK
PB
JX
HK
BM
BB
DB
EO
AL
FN
U
P
DZ
Average Tag
5.40
5.40
5.40
5.47
5.50
5.50
5.50
5.53
5.60
5.63
5.67
5.70
5.83
5.83
5.87
5.90
5.90
5.97
6.17
6.37
6.43 ft
6.60 ft
7.00 ft
7.23 ft
7.57 x
7.63 x
8.40 x
10.27 x
16.60 x
30.33 x
155.83 x
Lab
SM
QU
c
EL
QT
NO
AJ
TN
DE
JS
VI
JE
UP
QQ
FE
CJ
AZ
AK
NJ
SZ
LT
VA
JY
Q
PW
SD
UA
RD
QX
LR
EV
% responding labs Frequency distribution
10 II
_ - llllllv|l|
_
-6 ' . -4 ' -2 ' 6 +2 ' +4
Normalized deviation of the mean from the known value
a No data submitted TAG SYMBOLS
ft s Above control
0 s Insufficient data x = Determined to be an outlier II s Below control
;i
+6
limit
limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997 16/30
Radium-226
% responding labs Frequency distribution
10
0-UtrJ. , ._, , ! ^^f f ,j. ^r-"
-6 -4 -20+2+4 +6
Normalized deviation of the mean from the grand average
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
17/30
Radium-228
Statistical Summary 182 Participants
The known value of this nuclide is 5.0 pCi/1 with an expected precision of 1.3; the control limits
are 2.7 to 7.3; the warning regions are 2.7 to 3.5 and 6.5 to 7.3
98(53.8 %) Failed to respond .
2(1.1 %) Outliers
4(2.2 %) Out of control
but not an outlier
Statistic
. 68(37.4 %) Within all limits
Respondents
1O(5.5 %) In warning zone
but within control
Non-outliers
Mean
Std. Dev.
Variance
% Coef. of Var.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
5.24
1.65
2.74
31.60
4.72
0.14
5.03
0.67
0.02
Grand Avg 5.05
1.16
1.34
22.91
1.01
0.04
5.00
0.00
0.00
6(7.1 %) More than 3 norm. S.D. ป
1O(11.9 %) Between 2 and 3 norm. S.D.
5(53.6 %) Within 1 norm. S.D.
of known value
23(27.4 %) Between 1 and 2 norm. S.D.
-------
18/30 ESD-LV Performance Evaluation: Blind-A,
Radium-228
Lab
A
AE
AF
AH
AJ
AK
AL
Res. 1 Res. 2
3.4
4.3
6.2
4.1
3.2
6.0
3.5
"j~> ...-t ~, *tซ* f . -y:> * : ' !' ' ,"-"--" '
A&^^c^y^'S /
'*AR:f
,' ->;ซ" > - '.w*"? ป
<""/'"! ''V- ,/-'->>
'"'. ,;^a ,W-A<,.'. *,</,,<; f" *l $-M* '""/
5.5
3.3 ^
.y ' ''y-yy y
6.4
4.4
v~ , '* ? ' - \'" K*' ' *, ,
',-' '<-'" V- ',,-r&^'
,_; w, ,,,, , ,,;,, ->.,.. ;,-,v-"
"- '.yyy '"'yy,-
6.5
,ปv.- j.v\S:/>.ฃ. y w .. 'V"V,
"v< ^'yyyy;;;
""y, -f' '"-'"t't
4.3
, - 1 V *^-% " ""' ??.'-'>
5.8
* '-'ป !,".-' ,
'ซ. - :-~-r.: :
5.1
5.3
4.4
4.5
4.5
5.0
3.9
4.3
6.2
4.2
3.2
6.7
4.3
Y>S". i * "
*$'*&&>''.
; tซ?i>/":pf
Res. 3
4.3
4.5
6.5
4.1
3.0
6.2
_3:8_ f
t?S,-V' ""
^>\^->\, ,;
0^^i^"-'^
5.4
5.2
6.1
^-y.-'Ay^-
B.v3 '
%l%?f^
4.9
_4.3_
5.3
> %v*ei'4^-*.?<ป\''
<-S?-? J-V VX"^
^- s ^'*\S
5.4
S?>^
s;t% - ' *'
5.2
^3.8 _
-. " . s\Xx"
5.8
4.1
'-;vv3.T
;x;->V\'-j-i\';,
!--;,<-ฅ-ti'
-;f'! ;;;v
5.5
-^r!^
^ i^l^ %
_4.1 ^
h4 i ^'^
5.9
"'*:''":""
.5.0
4.7
4.6
4.0
6.1
3.9
6.1
6.3
7.0
>1-;^;S?/^;; '
..".'5:6.
U&- M>"v,rf,'
4.4
4.8
^ff^"' ', :"I"V
" J?,:8-
,v *^i7fw' :
4.9
. \ " i* -% , v
^s -* A" vo-;-'-.; '" '
5.0
4.4
'''' A:'-"''N> '
5.3
4.3
JV vV "* k tซ v? *; \^
,^-;: ซ>,-;;vV
.- .- ' '.,. f . j%\
*%$ *.^',,,
5.3
5::Hp^
J , -
'i>4-:/ \'T;
0.44
0.67
0.85
' V ",.. ,~ '' v.'~
0.17
, 4*?i\->~,,i~-
0.45
0.26
f'-:i^, '/} \ /-/r
0.93
x " ^ * r1-'
0.29
s ^ \JA " f
<''" '
" " "
0.25
0.55
$.[*
0.55
0.15
r ^
'^ *' * * v
' - , '- , - ''
0.64
r>'"T - _
0.20
s ^ ' " ^ '
0.21
0.32
0.31
0.15
0.25
1.14
0.61
0.409
0.091
0.136
0.045
0.091
0.318
0.363
'" y/ '/V^y
""V "',.",-:. '_',',-, '
-*< '- '?^y-;v
0.363
0.545
0.772
.' '-_x- --*,:>! -;ป
0.136
'"'s f "" -X %VK^
0.409
0.227
" '/r/'vT .-." \i'~
0.818
' * < w
0.227
' %^ *-% ^ %C> A %*' >
0.227
0.500
0.500
0.136
-'-' ^? '"'.''''
J" \ j""" '**'' * f.""
"'* '":" -1 *._, l^' ,* -
0.545 ^
-;.^,-yr-.--,y~
v __ ><
0.182
0.182
>
0.273
0.273
0.136
0.227
1.000
0.500
3.87
4.37
6.30
4.13
3.13
6.30
3.87
r-T^? K .^
4^y;;4^
^^:^yO-
5.60
5.53
6.13
/. "*:>ฃ&* -V
5.40^2^
^ ^--;fycr^ *
4.43
4.60
y^-^?!!
-1.58
-0.91
1.66
-1.22
-2.55
1.66
-1.58
jjrr ' JT^V-
t\%*^' - y\^
0:^5^5
0.73
0.64
1.44
^^\,y-?,^x-v ' A ,
JX4?J
A-V'^v"^'*
-0.82
-0.60
^\ "jl;^.-^ % v;'
5.03 -0.02
, (* itw*. yf^tf^fp ff.* tfttfttfUStfi ^ V' "\^XS
"";'*\-"\,-^:
5.07
^y;- .*;;; ~ฃ;
, ^"SS*V^'', " ^ "
' ^ " "" '-.-. "-^ '',
s "" - v *f '"'
\ s " v '\^ s
^5.77_
*,["$'
..*''.'' '''<.'
4.30
5.97
V ' '
4.87
5.03
4.57
4.27
4.83
4.60
TAG SYMBOLS
Determined
to be an outlier
0.02
s v^. vซ. "j; ' ซ. "ซ
?C.VV'^-
^^A s 5 ">^ ->\ ^ >
j; tftyK. ,y v\ f^V
0.24
-1.62^
'; ,v r'-- ,;';
1.04
%-l:04
.,., f.-. ^ *y^f '- *- i- "V s
^ " ^ /^"V "*' ''""-V
\- "^ 'ii\' ' s ^ ' ^ " * A *
v>AV< ;^' >sv"-#^- ** *
wO!53^
' *''; :'!'""' ;*x fx -
-0.75
-0.53
^':V. ^y-c*-^.
0.04
y , v* *y< * w^ i^ซ>* ซ*^ **. " ;' ^ -""X "- ^
f *' * ' v '. ป j /
\ ^v^-x^ ' s '%
;>v / v ^ซ, "?,'
0.31
-L55^_
v;X?ฅ -ปy.
1.11
-0.98 _
i ' "" v '\ H "- "*+ "\
/* f s " ' ; - " ;' ' ^ * *
/ AV ^ *'^.* * '' % V^
'' -- ^ ; / x*t; <
1.02
;;v":':"r'"ปF;
' ','"""- ^k--"
-0.93
v" ' '' \7 --,"
j1.
1.29
\ ft-' ^ f
V; ; y ^/ . /
- ':-,-. '
-0.18
0.04
-0.58
-0.98
-0.22
-0.53
control limit
control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
19/30
Radium-228
Lab
Exper. Rng anal Normalized deviation
Sigma (R + SR) Average (grand-avg) (known) Tag
^JBMBK-S^SO-: <->-" 'xVWJ- > ซปW > " ,' --
-Jin^CarV-^, ;'H^/> -\:;'Y"
*ป*!,%! ^ssv: -;^~ซ;;-,-:, ,-M.,,O -- -. v;j;
/ซ^>t;V<0 ,,', ^>*^^>!* ?ซ?-\-^ >,>, -\- :\
-**"i!l,r::v ,:<'"" V\fsฐ,,\ .xsi'SiV.' "'-:', .-'*ฐV^..
'JJ&; ^I^MSi ;%*s^-^
:';>S^-' v^*T-:;!t^f/^-v,^f-^>';
- LT? vv::l4;iv,;^,V4ฃr:v^ -. 12.9- -
M. ' 5.1^ _ 5.1 6.0_
0.682
0.045
0.273
0.318 5.97 1.22 1.29
vw.-twAVAgw.-s,, AS -As^tw^^s SAtw^wsr^V*^^^*^^^^ f(ซ5'ซ-.
-*. -^-::ir--c^^%'-^r^-i-;^^^^^v^^
~s" \.1 ^ , \ ".\, '^-!i-!\---f-*~^\-,"^st?,Jt^\V-;>o,;\ y\\*t
.' , ---,/->' -^; ; \^^:^i^^^:^^-
:-: ''- - v ;./:^&^i ฃ;\;;AS^V-^::^?
0.182 5.23_ .0A4^_.^.2^L,
> Xvv-K's,^*;
>ซ* !-. \N*ซ
L20
0.52
'MY'.
N
4.5 5.2
4.6 0.38 0.318 4.77 -0.38 -0.31
- S\S,
= No data submitted
0 = Insufficient data
TAG SYMBOLS
Determined to be an outlier
ft = Above control limit
It = Below control limit
-------
20/30
E8D-LV Performance Evaluation: Blind-A, 21-Oct-1997
Radium-228
Lab Res. 1
Exper. Rng anal Normalized deviation
Res. 2 Res. 3 Sigma (R + SR) Average (grand-avg) (known) Tag
0.57
0.20
0.500
0.182
4.63
5.50
-0.56
-0.49
0.909 3.50 -2.07
0.091 3.83 ,,,..,-1-62
1.259
4.13
-1.22
-2.00
-1.55
-1.15
OY 4.0 4.1 3.8 0.15
p f!L. J;? .,. ,4-2> - ฐ'6.8.
PB 5.0 5.2 5.0 0.12
0.091
5.07
0.02
0.09
PW
Q
QT
QU
QX
QZ
RB:
RD
5.4
5.6
7.8
2.5
8.7
4.4
fSIp:
6.2
5.4
5.9
6.4
3.0
6.4
4.7
si'ฃs>ฃ
6.2
5.6
6.3
6.8
3.5
0.12
0.35
0.72
0.50
0.091
0.318
5.47
5.93
0.55
1.18
0.62
1.24
0.636
0.454
6.9 1.21 1.086
4.4 0.17 0.136
^yx^^vjr-K-'-.-.f-" t " "v\*,t*f*ซ""""" *'.~ > > > "-"^- " ,
6.2 0.00 0.000
RU
RZ
S
sc
SD
SF
SO
SI
4.9
5.0
6.0
5.5
7.4
3.8
4.5
4.2
5.6
5.3
7.2
3.7
4.5
4.7
5.4
5.4
7.4
3.7
0.23
0.40
0.31
0.10
0.12
0.06
IT
0.045
3.73
-1.75
-1.69
0 =
No data submitted
Insufficient data
TAG SYMBOLS
x s Determined to be an outlier
IT & Above control limit
II = Below control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
21/30
Radium-228
Lab Res. 1
Exper. Rng anal Normalized deviation
Res. 2 Res. 3 Sigma (R + SR) Average (grand-avg) (known) Tag
0.818
2.124
2.384
0.227
2.903
W 5.0 4.8 5.1 0.15 0.136 ,_ 4.97_ jHL.-^< l9'ฐlw^
WE'- -ป>*^r"X <'7>T--' o?^v. >\v* :,^'-;-1' ",-,'"'?%fi' , /-;)v?^V',-- Jx'.^^^'^^H^^^'ft^Vu^!!^
WH 3.1 3.3 3.8 0.36 0.318 3.40 -2.20 -2.13
WO 4.2 4.1 4.0 0.10 0.091 4.10 -1.21 -1.20
WR 4.4 4.7 4.8 0.21 0.182 4.63 -0.56 -0.49
XJ
xk
XL
XM
5.3 5.3 5.3 0.00 0.000
3.5 4.5 3.3 0.64 0.545
5.30 0.33 0.40
3.17 -1.71 -1.64
= No data submitted
0 = Insufficient data
TAG SYMBOLS
x = Determined to be an outlier
tf = Above control limit
& = Below control limit
-------
22/30 ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Radium-228
Exper. Rng anal
Lab Res. 1 Res. 2 Res. 3 Sigma (R + SR)
^^f;#f 'Ifi^^^ : : :; -'-':;:
Normalized deviation
Average (grand-avg) (known)
- *;:t , - ; - J~ ; - > ~^^M|tf1^Jv|^^
Tag
!lf5*
Data sorted by Laboratory Average
Average Tag Lab
1.57 U JX
2.90 SX
3.00 QU
3.13 AJ
3.40 WH
3.50 NO
3.73 SI
3.77 XM
3.83 O
3.83 CA
3.87 AL
3.87 A
3.97 P
3.97 OY
4.10 WO
4.13 OF
4.13 AH
4.23 U
4.27 EB
4.27 CJ
4.30 DB
4.37 X
4.37 AE
4.40 FN
4.43 BH
4.50 QZ
4.57 E
4.60 EO
Average Tag
4.60
4.63
4.63
4.63
4.63
4.73
4.77
4.80
4.83
4.83
4.87
4.93
4.97
5.03
5.03
5.07
5.07
5.17
5.23
5.23
5.23
5.30
5.30
5.30
5.40
5.40
5.40
5.47
Lab
BK
S
WR
RZ
NH
TN
N
HK
JS
EL
DT
TD
W
DZ
BM
PB
BO
ID
L
C
TQ
UQ
XL
HL
SD
M
BC
UP
Average Tag
5.47
5.47
5.50
5.53
5.60
5.67
5.70
5.77
5.83
5.93
5.97
5.97
6.13
6.20
6.20
6.30
6.30
6.63
6.97
7.00
7.03
7.13
7.13
7.33 ft
7.33 IT
8.53 IT
12.80 x
12.90 x
Lab
T
PW
NJ
AZ
AW
SC
VI
CS
CE
Q
K
DE
BA
SZ
RD
AK
AF
JE
SM
QT
JY
ss
I
SF
QX
VA
GQ
LT
% responding labs Frequency distribution
10 U-
- Illlll-lllil
-6 ' -4 ' -2 0
-
+2 ' +4
I
+6
Normalized deviation of the mean from the known value
s No data submitted TAG SYMBOLS
IT = Above control
0 s Insufficient data x s Determined to be an outlier li = Below control
limit
limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997 23/30
Radium-228
% responding labs Frequency distribution
10
1 I I 1
-* -4 -2 0 +2 44 +6
Normalized deviation of the mean from the grand average
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
24/30
Uranium (Natural) Statistical Summary 182 Participants
The known value of this nuelide is 31.0 pCi/1 with an expected precision of 3.0; the control limits
are 25.8 to 36.2; the warning regions are 25.8 to 27.5 and 34.5 to 36.2
83(45.6 %) Failed to respond ;
5(2.7 %) Outliers
7(3.8 %) Out of control
but not an outlier
Statistic
. 78(42.9 %) Within all limits
Respondents
- 9(4.9 %) In warning zone
but within control
Non-outliers
Mean
Std. Dev.
Variance
%Coef. ofVar.
% deviation of mean from known value
Norm. dev. of mean from known value
Median
% deviation of median from known value
Norm. dev. of median from known value
29.53
4.57
20.85
15.46
-4.75
-0.32
29.63
-4.41
-0.30
Grand Avg 29.52
2.36
5.58
8.00
-4.76
-0.62
29.62
-4.46
-0.59
12(12.1 %) More than 3 norm. S.D.
9(9.1 %) Between 2 and 3 norm. S.D.
5O(5O.5 %) Within 1 norm. S.D.
of known value
n 1 and 2 norm. S.D.
-------
25/30
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Uranium (Natural)
Lab
A
AE
AF
AH
AJ
AK
AL
- AP>J
AR
. AIT/
AW
AZ
BA
BB
BC
BO
BH
BK
HT
BM
BN
BO
BS
BW
C
CA
CO
CE
CJ
do
CP
CS
CX
B
DB
DD
DE
DI
DO
DT
DZ
E
EB
EL
CO
Res. 1
30.4
32.7
29.0
28.2
39.4
32.6
33.4
y ""?T*'' ,*^
27.3
!-'"::'?3>>.>#
29.6
28.5
26.4
27.3
30.2
- ''' ,'t'i f, .> .
31.8
30.9
'! ' '*ป " *'\
29.6
17.1
29.0
_ y -\;
31.0
26.9
32.8
27.0
* '',' -', '"
30.3
34.8
v
24.3
27.5
31.1
27.5
24.4
28.9
26.8
28.1
Res. 2
31.9
33.4
28.0
29.1
31.5
32.3
33.5
^V^Tg^
26.7
^1|>?:^K?4
28.4
28.9
29.8
27.9
30.5
,,.% ',;ฃ' ,,'~*2xY, '
29.2
30.8
, c ^ *?ฃ ': \ ' "
29.5
27.8
30.1
** ' - "\-
' * '' , ^ : ' -
31.1
23.1
\5, 'r ;.!;; - 1
32.6
J!6,$L.
VT% ,pl^^;
ป'\- <'>, ,r'-
32.4
33.7
'-, ""'%'V "^
26.0
' \1 y"'
27.6
31.5
30.7
24.9
30.0
28.7
29.5
Res. 3
29.5
31.8
27.5
29.3
32.2
31.1
, If 6
26.8
<. ,'* / V^ ^ii*
29.3
30.7
28.6
27.6
29.8
' >, ':< '' ,'ซ \
Vv(, ,' 1-1-
31.8
30.7
' ^ v ^_' ^ i
31.3
23.1
30.2
- - s/
-! , -, >~~ >-"
30.3
25.4
32.0
27.0
v jr'^'-rv
'.--r'-,->V
31.5
35.5
- ' r ,.
23.6
,'V- -'v.
28.7
30.7
31.7
25.7
30;5
25.5
30.8
= No data submitted
0 =
x =
Exper. Rnganal
Sigma (R + SR) Average
1.21
0.80
0.76
0.59
. 4.37
0.79
0.67
1x>* "! "
0.32
;.- '* ' -x -
0.62
1.17
1.72
0.30
0.35
. : .
1.50
0.10
1.01
5.36
0.67
0.44
1.91
,"7"-
0.42
0.58
'* ;
.' %It ' '
1.05
0.91
't-
1.23
0.67
0.40
2.19
0.66
0.82
1.61
1.35
0.473
0.315
0.295
0.217
2.058
0.295
0.236
; -'* :/:'^V v Xjt
30.13
22.67
29.77
.'; - ^ '<. '
, J1* *" ^^^ ^ l%
-' '".-ซ<'
30.80
25.13
. ^ .... ........ s*-.- f-^'r^
32.47
26.67
, , '.'.*
31.40
34.67
24.63
27.93
31.10
29.97
25.00
29.80
27.00
29.47
TAG SYMBOLS
Determined
to be an
outlier
Normalized deviation
(grand-avg) (known) Tag
0.62
1.80 .
-0.78
-0.38
2.80
1.43
2.49
lXoiV::'-xH
-1.50
:;\C;^1:V ^?
-0.24
-0.09
-0.73
-1.11
0.37
}^J^;^'1''^;;'V
0.81
0.74
V's ^ - \ ^ *'
0.35
-3.96
m 0.14
}\l^^' *- ;-V'
\\ X "A* v',X ' " -'-
0.74
-2.54^
%i " "x** " "v '-s';
1.70
:1.66_w _
";;>: \'4K/":"
"^ !" "" f * ^ " ' *, '*'"' f
1.08
2.97
.. V-;* ' ,,-
-2.82
-0.92
,^
0.91
0.26
-2.61
0.16
-1.46
-0.03
IT = Above
!) = Below
-0.23
0.94
-1.64
-1.23
1.94
0.58
1.64
1 -; i - 1*Vr;',; 1 ,"
-2.35
n-'.'"".-.^
-1.10
-0.94
-1.58
-1.96
-0.48
i?:A "'--,'. -ป:>^
-0.04
-0.12
:+'< . ':'yv'i/. '
-0.50
-4.81 1).
-0.71
:,-'-- ''\ ,*"
^v-^vSp'' '* "'---
-0.12
-3.39 _ll
';*\';v ' * '
0.85
-2.50
-'"""" s^\^.' #,_/
1 , ;.,,,,,,, - - -
0.23
2.12
'' * ,
-3.68 li
- "T " _
-1.77 _
--:
0.06
-0.60
-3.46 $
-0.69
-2.31
-0.89
'' - ' '# ,
control limit
control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
26/30
Uranium (Natural)
Lab Res. 1 Res. 2
Exper. Rng anal Normalized deviation
Res. 3 Sigma (R + SR) Average (grand-avg) (known) Tag
rui az.u 31.0 32.0 0.58 0.197 31.67 1.24 0.38
^v f. ^JJ^^^%s^^^^s^A^A^^v*(Aซ^AW^v^^w^^^o.^^^sv^^^,JW(J{- V^^VAV-VAVV,^ s-.^ ^ww, (.^v^s v % vi*.w.^%t .-SK s ,-.%;.% ^ ^^v.v, ^ ^vj-sv,^-.^^-^^,^ (V-.sw w. ^ ^V.A\\J- sjw.vy^v ww.^ v^ s^i?^^A;Wsw;^^'-i^^'1X^ ^ ^MW^
ir.i oo n QO i QO i ft rws n r\or\ 32.07 1.47 0.62
32.1 0.06 .020
28.87 -0.38 -1.23
0.35 0.138
1.17 0.433
0.09 -0.94
0.89 0.335
0.51 -0.35
5.55 3.221
0.35 -0.50
2.55 1.008
32.1
30.0
30.8
29.0
33.8
31.6
1.50 0.591
1.31 0.512
32.23
1.56
0.71
30.20 0.39 -0.46
0.10.;., .-.-0.089
= No data submitted
0 s Insufficient data
TAG SYMBOLS
Determined to be an outlier
ft & Above control limit
U- & Below control limit
-------
27/30
ESD-LV Performance Evaluation: Blind
-A, 21-Oct-1997
)
Uranium (Natural)
Exper. Rng anal
Lab
NA
NJ
NK
NO
JV"* y /
' O,' /'*ซ
OB
J>F;:^
OM^
OS
"'fMT-^
< ^^iam1-- >,..'iS*t-'' '" y'-i&Z
"^'$^~:~f^f-fi
30.7
'^i^T^'-'Sil
s /"xfe*1* ' 's -*;'/ __,ซ*%"*
25.7
22.3
'* f; Xฃ ^V\'('!!>'W-JV> 'f
3L6
' * V' - > >-" "" W s 'w '' ',;' "
30.0
f .' ' ^ * -. " -.*~"
C" '. ""''.I'.' , \'
*' ~: '--''.' /"^
24.6
32.7
27.0
'> "" \* "" ซ.. ''^' /''"
30.9
1 ":,;ป' >V>V ' "!*?"'
25.3
- \^ < ?^\ ' >"*
30.9
28.4
"; s -,v_ %' -./
"*::>'> -i-"1 v "" ^ _
/"vV-, rt gฃ
''' ' '"""i" \ ' X "]> ^^
- '- %! ,," x-'"'
30.3
'* '-,> - - -
27.9
28.2
''""- 'v - '
28.0
28.2
36.4
28.6
25.5
30.2
Res. 2
32.0
29.4
29.1
29.3
./^ " ,/&$ v ' '*
/fti '^x* ^ ^" ''
J_3p.4^
^IMI^
svVs^&V*
i- : v^&^t^
28^8
<>^ -.""^"'xt^-^j:'5'
^ t< '^'X^'. f'^j^VS'1:
24.4
33.0
' x - 'p^'^^-^C
32.8
O \* ^"s% \^ "'^
29.9
"vf1 fe >-,'*' ^'
y J ; '"'' ' -/' "
'-, \"'^ "" J,s j.^'1'1'
23.2
33.3
,.27:0m.
:/''^'':vJ
30.0
;- , 'f'^i ป'ป
25.6
H'^iP-,
33.1
30.9
< **?'*"*&' **ฃ$?* "
"J','. **?' '"
28.3
29.5
27.1
27.7
33.8
28.3
24.9
..-. .V 4: '
30.5
Res. 3
30.0
26.3
29.0
29.9
' ; " * \f 'f"'^f Y/" \5'--i-
/^l;--^; ' ; ,-'
30.4
^^Iffi'?'
S^^^-r
"""\29.0_,
, r^^^^^/V^'^XI:.'
yXl^U1-,^^ c> v
**>' ^Sj :?! \^=\'J- * &**; ^
24.6
28.8
V. , ^,^V.^W^,V^. *.;,* f
33.3
'*'\ ^ "" s ^ /% X \ X ' *" ""
31.1
.ฃ t'/t "-V S- -'
^ " * ^^ ^ ^ ^ ^ . /....
-^ ^ \;|;, ss " \
21.2
32.3
27.2
f. yt f ff^ f : f f. -.^
*--\t s "- *' , if
33.6
;H/^!>" ' ฐ:\<"~-"~
27.1
?'ฃ*ฃ&&'':
32.2
^28.8 _
'\ f ^ft ^ * " '^ f * " ? *
" V\V>-'' ' ' ""V"1" ^
.. :,/,,-''"' ^Q.B^-
vvji ^ ^'''*CV.V ^ f "" %^ ^
^-"j :--'-' v
30.1
X%s* '" ' ' ' '
28.2
29.7
'''
5, ^ " ^ ^ ^
v .... , , .-
27.0
28.3
32.8
29.0
25.7
> " , ' --
30.9
No data submitted
x =
Sigma (R
1.15
2.02
0.15
0.70
.. ">" ' ' i A ^
lA-^;- 'V* " - * * -
0.01
ji*>'"'f-^"" - "--'
;tt^y.Vfl-\t?
1.04
P"'- ,.-;",y|.i7s
' / ^ * , '\v"X ../\ ' ^ f
0.70
5.39
^ ^ ^ , ....^,.v................ , , ^ ,
0.87
' " v -' * , ' ' ' '
0.67
^ 'V ,_,.
S "' " -.''^ '
>' ' '''"
1.71
0.50
0.12
;;.&"?..< , ' ' ,..
ซ 1-87
;,.x 0.00
AV. '" ''
^-, -'
0.15
^* %
0.21
0.81
' rซ"
0.55
0.32
1.86
0.35
0.42
-. ;-. L
0.35
+ SR)
0.394
0.748
0.059
0.276
; ,C .//,. ''" *%ฃ''* ^
**tC
" 5 ,,s ^.;'i
i^T.-^.C-;
0.374
i^Tr^^v^
' "\ ^ " ^ "\X"1'i2
0.256
3.108
SV"*"' "'y'-'-i 0" ":
0.335
Av^ "* ' 's1-
0.236
> " s s*
,. " S % ] .^ . H?
,'"'ซ ;- -"-,;
0.669
0.197
0.039
""' ^ V"vCVKf '
0.709
" '"Jl':''' ^
0.354
, .'< 4;, ,\ '-,
0.433
0.492
, V.V.ฃ.A %
^ , v ' " "''" "
"""" ";
0,000
" ' A-,* W
0.059
0.079
0.295
0.197
0.118
0.709
0.138
0.158
0.138
Average
30.67
27.10
29.13
29.23
^'" ^ *V* * '-, '-, ^ \^ซ
N\Cf F^- V^X
30^40
' W.;v'^'>.^^> ^
^y^ ''^**
' -^x:
29.50
: 's^f^^^
/ ^ " ' '"'^ ''^
24.90
28.03
" f\"^*' ' '
32.57
, v '^ ' -..*
30.33
' X V'V/^ s
' ; ?*&*. ^'- " ^
;< " - ;'^'^
23.00
32.77
27.07
*' v - ^ - -^
, ,'V,S^-">" --?'--'"'><-! %'f1 ' '''",' v,- . >"s
?' >- :>s"r ป ;V ';'v ^"-"- '" ' 's'il\'"! *^ 'ป
-b.oi
r'-^f'?^T\^4:
^ \\ "" A ^ . * "^ ^ /"^k!1..
-2.67
-0.86
^%s ^. .ซ...,^.^ "'|^*'i>.' -.v,"\.f^
"i.76^"
; <- s ; ^ > * '
0.47
, wwy-y... v ^ ^ "%"" t1",, ^
s w ^ >vr^>V"^'"
-3.77
1.87
-1.42_
-^-ihlฐ ?=;,"' v"-^.
,wrjM?v >*---
"/.\, <^ , -\<, ^'
-2^03
^-X-C-vV--^ ^
1.47
:0:09___
'^ f ^ f "
^ ' ^ " ^ A % "" "
" >16,68;j;> -'"
~\.^ '' '' . '' ''
{ป ' - \/-^--:'"' !
_0.35_
1 , - '<-
-0.80
-0.23
'''"< -- , -!.'";'
-1.25
-0.84
2.78
-0.51
-2.40
0.58
ft = Above
11 s Below
-0.87
f '*""'; f$jฃ'"i"'"
^ ' > ซ"J -. ^
-3.52 II.
-1.71
^"V^vY ป%.-.JJ-.-H^ :*, ";'-;
0.90
x* y . o "^/^ ^ *;v ^
-0.38
;. V0 w%^ *,ซ./. A^ v.^w.,^^h ^
, ' V '' >>!^.?'^S-5*''''/f^t
ife'-i''^^
-4.62 li
1.02
w-2.27 (
s"1' ^ '' ' ., " / ' ' 'V\ . ""
f\ *?O
; ' r:T- " '* '",*
2OQ
OI7
K\:-- -;-,%7^ : -
0.62
-0.94 _
!, - -"^ V" ',' '
. .." s '
>17.44v";';~x?p/
.' .' ....' .v.x ^ ^
ป'-!,'/ *-;'"';
^^,__,ซ
-, i. ^ -/
-1.66
^-1.08(__
'-,' ~^->|r'"-v *i-'-ฐ
"* ' "\ ' *:"" ;'
-2.10
-1.69
1.92
-1.37
-3.25 Ji
-x - ' ซ
-0.27
control limit
control limit
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
28/30
Uranium (Natural)
Lab Res. 1 Res. 2
Exper. Rng anal Normalized deviation
Res. 3 Sigma (R + SR) Average (grand-avg) (known) Tag
SM
SO
SS
&K
SZ
T
30.3
"^'
" v *',
28.3
\ -.-ซ-* AW AV.S.S ,
^ ; - *-
30.0
28.9
28.9
26.6
32.0
30.6
26.3
*. w Ns. % - ^ s o
f^S^C
30.1
29.3
29.5
31.0
31.6
30.7
"'- - ' ' "' -
,\?.\
28.6
v ^ s ^ ^ ^
x ^H *S
30.1
30.2
30.5
30.1
32.4
0.21
r ;-^
,
1.25
^. A % -. * - v
- ;> -
0.06
0.67
0.81
2.32
0.40
0.020
0.256
0.315
0.866
0.158
30.07
29.47
29.63
29.23
32.00
0.31
-0.03
0.06
-0.17
1.43
-0.54
-0.89
-0.79
-1.02
0.58
VO
'Y^
W
28.6
30.8
^r
28.2
29.1
31.3
iS^
28.9
28.7
29.7
^^
27.9
WH
wo
WR
35.2
28.8
29.6
rtiW-'-'.s V* V*. wtrti* v,\C ^ s %
31.2 32.0
26.6 27.7
29.6 29.9
0.26
0.82
V V ',.'.
0.51
2.12
1.10
0.17
0.098
0.315
0.197
0^788
0.433
0.059
28.80 -0.42 -1.27
; -xxx^x-j-^- - * '->-> - v -x^? y? *<>,ฃ? " '>^Sfr"V^sKv-
'.: ,*,> v\^^:^;v^ -,.; vV^,V^^K^X^^-*:
-0.23
-1.54
30.60 ^ N 0.62
^ S'
28.33
32.80
27.70
29.70
-0.69
1.89
-1.05
0.10
1.04
-1.91
-0.75
= No data submitted
0 = Insufficient data
TAG SYMBOLS
= Determined to be an outlier
tt s Above control limit
II = Below control limit
-------
29/30 ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997
Uranium (Natural)
Lab Res. 1 Res. 2
YM , , ,^ -^ ?,-,, ,;\ ;,<:/.; <:'-,;
4^-^^^^.^r
Exper.
Res. 3 Sigma
V;4,,;,,-s -, \\~-
""?-'"' -5* r*' ' ,!,
Rng anal Normalized deviation
(R + SR) Average (grand-avg) (known)
'' - .':--. ---,',-''- ', *s- '^*.^>VsV&V?-x^^i^^/.^i>4,
' ' .'"'"^ ^.^\^^:^^^^
Tag
&i<*, IV
o ' i:^>
Data sorted by Laboratory Average
Average Tag
0.80 x
19.00 x
22.67 U
23.00 li
24.63 U
24.90 U
25.00 U
25.13 U
25.37 U
25.90
26.00
26.67
26.93
27.00
27.07
27.10
27.37
27.60
27.70
27.73
27.93
27.93
27.97
28.03
28.07
28.13
28.17
28.27
28.33
28.33
28.63
28.80
28.87
s No data submitted
Lab
RD
M
BN
PW
DB
OY
DZ
CA
SF
K
QU
CJ
AR
EB
QM
NJ
RZ
BB
WO
SO
UP
DE
U
P
S
RK
AF
BA
W
KT
SD
VI
GQ
Average
28.87
29.07
29.10
29.13
29.13
29.23
29.23
29.37
29.37
29.37
29.47
29.47
29.47
29.50
29.57
29.60
29.63
29.63
29.70
29.77
29.80
29.97
30.03
30.07
30.13
30.13
30.13
30.17
30.20
30.33
30.40
30.40
30=53
Tag Lab
AH
JE
AW
RP
NK
NO
T
QZ
HL
AZ
XL
sx
EL
OS
XA
ER
X
SZ
WR
BO
E
DT
VA
ss
RG
JN
BM
BC
LF
PG
OB
I
SM
Average Tag
30.53
30.60
30.60
30.67
30.70
30.80
30.80
30.93
31.10
31.33
31.40
31.50
31.67
31.97
32.00
32.00
32.00
32.07
32.07
32.23
32.47
32.57
32.63
32.67
32.77
32.80
33.83
34.33
34.37
34.67
38.67 x
40.43 x
49.17 x
TAG SYMBOLS ft = Above control
x s Determined to be an outlier & = Below control
Lab
SI
vo
A
NA
JY
C
BK
BH
DO
XM
cs
QQ
FE
TQ
TD
JS
AK
QX
FJ
L
CE
PB
AE
ID
Q
WH
AL
SC
AJ
CX
FN
HK
Nfl
limit
limit ]
-------
ESD-LV Performance Evaluation: Blind-A, 21-Oct-1997 30/30
Uranium (Natural)
% responding labs Frequency distribution
10-
*
U
-6 -4 -2 0 +2 +4 +6
Normalized deviation of the mean from the known value
% responding labs Frequency distribution
10-
oJซ*
-6 -4 -2 0 +2+4 +6
Normalized deviation of the mean from the grand average
------- |