MIDWEST RESEARCH INSTITUTE
MRI
EPORT
SOURCE TESTING REPORT
EMB Project No. 73-FRT-l
ARCO Chemical Company
Fort Madison, Iowa
Midwest Research Institute
Kansas City, Missouri 64110
EPA Contract 68-02-0228, Task 22
MRI Project No. 3585-C, Task No. 23
MIDWEST RESEARCH INSTITUTE 425 VOLKER BOULEVARD, KANSAS CITY, MISSOURI 64110 • 816561-0202
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MRI WASHINGTON, D.C. 20005-1522 K STREET, N.W. • 202 293-3800
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SOURCE TESTING REPORT
EMB Project No. 73-FRT-l
ARCO Chemical Company
Fort Madison, Iowa
by
E. P. Shea
Midwest Research Institute
Kansas City, Missouri 64110
EPA Contract 68-02-0228, Task 22
MRI Project No. 3585-C, Task No. 23
MIDWEST RESEARCH INSTITUTE 425 VOLKER BOULEVARD, KANSAS CITY, MISSOURI 64110 • 816561-0202
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PREFACE
The work reported herein was conducted by Midwest Research Institute
(MRI) pursuant to a task order issued by the Environmental Protection Agency
(EPA) under the terms of EPA Contract No. 68-02-0228. Mr. E. P. Shea served
as the Project Chief and directed the MRI field team consisting of Messrs.
Henry Moloney, Acid and Water Sampler; William Maxwell, Engineering Technician;
Reid Flippin, Testing Engineer; Michael Bechtold, Engineering Technician; and
William Cunningham, Laboratory Technician. Mr. Winton Kelly, EPA, was Project
Officer and Mr. Lee Beck was the Field Engineer responsible for collecting
process data. Mr. E. P. Shea prepared this final report.
Approved for:
MIDWEST RESEARCH INSTITUTE
Paul C. Constant, Jr.
Program Manager
ii
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TABLE OF CONTENTS
Page
I. Introduction 1
II. Summary of Results 2
III. Process Description and Operation 9
IV. Location of Sampling Ports 11
V. Sampling and Analytical Procedures 13
A. Fluorides 13
B. Ammonia 15
C. Integrated Gas Samples ..... 15
Appendix A - Fluoride Results. 18
Appendix B - Gaseous Results 29
Appendix C - Operations Results 36
Appendix D - Field Data 38
Appendix E - Laboratory Report ........ 75
Appendix F - Test Log 104
Appendix G - Project Participants and Titles 106
iii
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LIST OF TABLES
Table
I
II
III
A-I
A-II
A-III
B-I
B-II
B-III
C-I
F-I
Title
Page
Summary of Results - Total Catch 4
Weight Results - Fluoride Runs
Analysis Results - Fluoride Runs
Fluoride Emission Data 19
Example Fluoride Calculations 20
Fluoride Data and Calculated Values 24
Summary of Results - Ammonia 30
Ammonia Emission Data 31
Ammonia Data and Calculated Values 32
Production Rate 37
Sampling Log 105
Figure
LIST OF FIGURES
Title
DAP Plant Effluent Stack and Platform.
Page
12
2 Location of Liquid Samples 14
3 Integrated Gas Sampling Train 16
iv
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I. INTRODUCTION
Under the Clean Air Act as amended, the Environmental Protection
Agency is charged with the establishment of performance standards for station-
ary source categories which may contribute significantly to air pollution. A
performance standard is a standard for emissions of air pollutants which reflect
emission limitations attainable through the best emission reductio.n systems that
have been adequately demonstrated (taking into account economic considerations).
The development of realistic performance standards requires accurate
data on pollution emissions within the various source categories. The objec-
tive of this project was to collect the data on .emissions of fluoride and am-
monia at a diammonium phosphate fertilizer plant. The ARCO Chemical Company
plant at Fort Madison, Iowa, was designated by EPA as representative of a well
controlled plant and was therefore selected for the emission testing program.
This report presents the results of the tests run at the fertilizer plant to
determine the fluoride and ammonia emissions.
On Monday, 19 March 1973, the equipment and personnel arrived at the
site. The platform erection was not finished. On Tuesday, 20 March 1973, the
equipment was unloaded at the stack and the laboratory. The support rails were
installed on Ports 1 and 2, but not on Ports 3 and 4. The platform uprights
used to fasten the support rails were not located properly and ARCO maintenance
people had to be recalled to change the uprights. A preliminary velocity and
temperature traverse was run Tuesday on Ports 1 and 2. The moisture determina-
tion run was not successful, so an assumed moisture value was used in setting
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up the nomograph for Run No. 1 on Wednesday, 21 March 1973. The assumed value
of 20% was about three times the actual moisture. This erroneous assumption
resulted in Run No. 1 having an 88.6 isokinetic value. The other four runs
using a 7% moisture value had isokinetic values of 98.3, 103.2, 100.9, and
105.3
On Tuesday, 20 March 1973, we were informed by the project officer
that sampling for ammonia was to be conducted if possible. We had enough
equipment to do this and we were able to get sulfuric acid from ARCO so we
ran five tests for fluoride and four additional tests for ammonia. The re-
sults of these tests are included in this report. The samples were collected
and packaged in polypropylene sample jars and given to the project officer
for delivery to the EPA analytical laboratory.
On Friday, 23 March 1973, we ran three tests—one fluoride, one am-
monia, and one integrated gas sample--removed the equipment from the stack,
-loaded the truck, and cleared the site. On Saturday, 24 March 1973, the crew
returned to Kansas City.
II. SUMMARY OF RESULTS
Table I presents a summary of results from the fluoride runs. The
fluoride caught in the cyclone ranged from 0.00 to 0.2 Ib/hr with an average
emission of 0.108 Ib/hr. The fluoride per ton of P20c ranged from 0.0 to
0.0123 Ib/ton with an average of 0.007 Ib/ton. The fluoride detected was
present in the soluble form in the cyclone catch from all five runs. The
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analysis for insoluble fluoride showed less than 0.06 rag which is the lower
limit of detection for the analytical method used.
Total fluorides caught during each of the five emission tests are
in Table I. As was the case in the cylcone catch, only soluble fluoride
was detected from all runs except No. 4. In Run No. 4 there was 0.08 mg
of insoluble fluoride detected. The total fluoride emitted ranged from
0.39 Ib/hr to 0.85 Ib/hr with an average emission of 0.554 Ib/hr of
fluoride. Table I also shows the emissions per ton of P,0 processed.
£ J
It ranges from 0.0758 Ib/ton to 0.0555 Ib/ton with average of 0.0356 Ib/ton.
Table I shows also the results of the moisture and Orsat analysis
of the stack gases for each fluoride run. The moisture varied from 5.4%
to 7.5% with an average of 6.5%. There was no detectable CO present. The
C02 content of the stack gas varied from 0.2% to 0.6%, with an average of
0.34%. The average oxygen content for the five runs was 20.58%, with a
variance from 20.2% to 21.0%.
Table II shows the weight of fluoride collected in each emission
test. The data as presented show the soluble and insoluble fluoride caught
in the cyclone and soluble and insoluble fluorides in the total catch.
The analytical results for the scrubber liquid samples, the feed
and product samples, are presented in Table III.
For the four ammonia runs, the analytical results show that there
was no detectable ammonia discharged from the DAP stack during the test
period. All of the analyses show < 0.3 mg of ammonia. The lower detection
limit for the analytical method is 0.3 mg of ammonia. Using the average
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TABLE I
SUMMARY OF RESULTS - TOTAL CATCH
NAME DESCRIPTION
DATE OF RUN
OS STK FLOWRATE, DRY,STD
-QA ACTUAL STACK FLOWRATE
PMOS PERCENT MOISTURE BY V
-PC02--- PERCENT C02 BY VOL, D
P02 PERCENT 02 BY VOL» DRY
- PCO PERCENT CO BY VOL, DRY
PROCESS FEED RATE
-FLUORIDES -- CYCLONE CATCH
CAN
.CAT.
CAW
MT
CAO
CAU
CAX
1C
FLUORIDE WT-CYCLONE "
FLUORIDE LOAD-PTL.STD CN
FLUORIDE LOAD-PTL,STK" CN
FLUORIDE EMIS-CYCLONE
FLUORIDE EMISSIONS
FLUORIDE WT-TOTAL
FLUORIDE LOAD-TTL,STD CN
FLUORIDE LOAD-TTL,STK CN
FLUORIDE EMIS-TOTAL
FLUORIDE EMISSIONS
PERC IMPINGER CATCH
UNITS
CN DSCFM
ACFM
L
Y -
TONS P205/HR
MG ....
GR/DSCF
GR/ACF
LB/HR
LB/TON P205
MG
GR/DSCF
GR/ACF
LB/HR
LB/TON P205
IF
03-21-73
135060
156408
6.5
.3
20.5
0.0
14.0
-. .50
.00012
.00011
.14
0.01
1.70
.00042
.00036
•49
0.035
71.4
2F
03-21-73
142550
165428
6.6
.6
21.0
0.0
15.3
.70- -
.00015
.00013
.18
0.0117
3.30
.00070
.00060
.85
0.0555
78.8
3F
03-22-73
129498
151009
6.5
.2
20.2
0.0
18.2
...... .10
.00002
-. .00002
.02
0.001
1.90
.00042
.00036
.47
0.0258
95.7
4F
03-22-73
138549
158642
5.4
.4 -
20.6
0.0
16.2
.80-
.00017
.00015
.20
0.0123
2.28
.00048
.00042
_.. -57
0.0351
64.9
5F
03-23^-73
116248
135750
7.5
.2-
20.6
0.0
14.6
0.0
^_
__
0.0
1.60
.00039
.00033
.39
0.0267
100.0
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TABLE II
WEIGHT RESULTS - FLUORIDE RUNS
Run
Number
IF
2F
3F
4F
5F
Cyclone Catch Weight
Soluble Insoluble
Fluorides Fluorides
0.5
0.7
0.1
0.8
-- __
(mg)
Total
Fluorides
0.5
0.7
0.1
0.8
__
Soluble
Fluorides
1.7
3.3
1.9
2.2
1.6
Total Weight (mg)
Insoluble
Fluorides
--
--
--
0.08
» w
Total
Fluorides
1.7
3.3
1.9
2.28
1.6
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TABLE III
ANALYSIS RESULTS - FLUORIDE RUNS
Run
No.
IF
2F
3F
4F
5F
Sample
Identification
No.
503
504
505£/
506
507
508k/
509
510
51,5,.
516
517
518
519
520
521
522
527
528
529
530
531
532
533
534
537
538£/
539
540
541
542
543
544
545
549
550
551
552
553
554
555
556
Description of Sample
Venturi scrubber inlet liquor (267. H3P04)
Venturi scrubber outlet liquor (267. H3P04)
Gypsum pond water
Reactor--granulator afterscrubber outlet
liquor
Cooler afterscrubber outlet liquor
Drier afterscrubber outlet liquor
Feed Acid (547. H3P04)
DAP product
Venturi scrubber inlet liquor (26% H3K>4)
Venturi scrubber outlet liquor (26% H3P04)
Gypsum pond water
Reactor—granulator afterscrubber outlet
liquor
Cooler afterscrubber outlet liquor
Drier afterscrubber outlet liquor
Feed Acid (547, H3?04)
DAP product
Venturi scrubber inlet liquor (267. H3P04)
Venturi scrubber outlet liquor (267. H3PO4)
Gypsum pond water
Reactor—granulator afterscrubber outlet
liquor
Cooler afterscrubber outlet liquor
Drier afterscrubber outlet liquor
Feed Acid (547. H3P04)
DAP product
Venturi scrubber inlet liquor (267. H3P04)
Venturi scrubber outlet liquor (267. H3P04)
Gypsum pond water
Farm runoff water
'Reactor--granulator afterscrubber outlet
liquor
Cooler afterscrubber outlet liquor
Drier afterscrubber outlet liquor
Feed Acid (547. H3P04)
DAP product
Venturi scrubber inlet liquor (267. H3P04)
Venturi scrubber outlet liquor (267. H3PC>4)
Gypsum pond water
Reactor--granulator afterscrubber outlet
liquor
Cooler afterscrubber outlet liquor
Drier afterscrubber outlet liquor
Feed Acid (547. H3P04>
DAP product
Total
Fluorides
17.3 gm/i
13.8 gm/i
1.7 gm/i
1.8 gm/i
£H
Ammonia
0.52
2.93 100.8 gm/i
592.6 mg/i
504.1 mg/i
12.1 gm/i
26.4 tng/gm
26.6 gm/i
17.8 gm/i
1.8 gm/i
1.7 gm/i
1.9 gm/i
1.8 gm/i
15.2 gm/i
26.0 mg/gm
25.6 gm/i
6.0 gm/i
2.0 gm/i
1.6 gm/i
1.7 gm/i
1.7 gm/i
14.5 gm/i
24.4 mg/gm
25.8 gm/i
1.8 gm/i
1.1 mg/i
1.7 gm/i
1.8 gm/i
1.7 gm/i
14.7 gm/i
26.0 mg/gm
27.5 gm/i
7.2 gm/i
1.8 gm/i
1.8 gm/i
1.8 gm/i
1.7 gm/i
15.5 gm/i
25.7 mg/gm
850 gm/i
520 mg/gm
2.7 gm/i
800 gm/i
470 mg/gm
2.8 gm/i
790 gm/i
500 mg/gm
2.8 gra/i
14.5 mg/i
750 gm/i
480 mg/gm
2.8 gm/i
730 gm/i
460 mg/gm
211.2 mg/gm
0.033
1.78 86 gm/i
1.65
449.6 mg/i
463.0 mg/i
828.0 mg/i
197.5 mg/gm
0.28
5.38 107.5 gm/i
1.75
487.1 mg/i
1.3 gm/i
580 mg/i
228.2 mg/gm
0.37
1.73
115.8 mg/i
599.5 mg/i
1.3 gm/i
201.0 mg/gm
0.35
5.18 111.3 gm/i
1.73
910 mg/i
630 mg/i
630 mg/i
204.4 mg/gm
a/ Sample lost during shipment.
b/ Sample missing.
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standard volume sampled, 44.135 DSCF and 0.3 mg NH3, the concentration of
ammonia is < 0.337 ppm.
Example Calculation
Ave VMSTD = 44.135 DSCF
Wt NH3 = < 0.3 mg
DSCF x 0.0283 = MM3
Mol. Wt NH3 = 17
Oil-SB = o.2367 mg/NM3
44.135 x DSCF x 0.0283 NMJ/DSCF
NM3 x 24-2— = ppm
Mol. Wt v*
0.2367 mg/NM3 x 24.2 m < 0.337 ppm
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During the first fluoride run it was discovered that Point No. 3
in Port No. 2 was a dead spot. At first it was thought that the pitot tubes
and lines were plugged. The test was stopped and the lines examined, but
nothing was found. No AP reading was observed at this point. The project
officer consulted with the ARCO people and they confirmed that they indeed
had a dead spot in the stack. We moved an inch away and finished the run.
On all future runs we stayed an inch away from Point No. 3 in Port No. 2.
On a process weight basis, the results of the five test runs range
from 0.026 to 0.055 Ib F/ton P205 and average 0.036 Ib F/ton ?2°5'
In an attempt to compare the effectiveness of a spray-crossflow
packed scrubber using fresh water with one using gypsum pond water, one of
the five test runs was performed while one of the three packed scurbbers was
using farm runoff water (not contaminated with fluorides) as the scrubbing
liquor. Two such samples were to be taken, but due to process equipment
failure, the collection of only one was possible. The result of this test
run (Run No. 4) was 0.036 Ib F/ton P205- Tne average of many tests performed
while one scrubber uses farm runoff water should be lower than the average
of many tests performed while all the scrubbers are scrubbing with pond
water contaminated with fluorides. The result of this single sample is not
sufficient for a valid comparison and no conclusion can be made.
The sampling train for all five test runs was modified to include
an unheated cyclone between the probe and the impingers. This modification
was made in an attempt to indicate the relative amounts of pond water mist
and/or other particulates in the sampled gas stream. The cyclone catches
8
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contained from 0 to 0.013 Ib F/ton P205, which is from 0% to 357» of the
total fluoride catches. Run No. 4 (using farm runoff water) yielded the
highest value. If a significant quantity of fluoride contaminated mist is
present in this plant's gas stream, the least amount of fluorides would be
expected in the cyclone catch of Run No. 4. That this test did not yield
the lowest percentage of fluorides captured in the cyclone, indicates that
fluoride contaminated mist is not an appreciable portion of the total fluoride
emisssions at this plant.
Both changes, the sampling of the plant while one of the scrubbers
was using farm runoff water and the inclusion of the cyclone in the sampling
train, were attempts to show strong trends in the amount of particulates in
the gas stream and the effect of scrubbing fluorides with fresh water. The
results fail to indicate any strong trends. A complete analysis would re-
quire different methods and more samples.
III. PROCESS DESCRIPTION AND OPERATION
The diammonium phosphate (DAP) facility at ARCO Chemical Company,
Fort Madison, Iowa, is designed to produce 750 tons/day of product (345 tons
P20c/day). Normal operation is at the design rate.
At this location ammonia is reacted with phosphoric acid in a pre-
neutralizer or reactor. Sulfuric acid is also added to the reaction mixture.
The slurry from the reactor is fed to a granulator along with recycled off-
size product and recovered dust. Additional ammonia is added in the
granulator. From the granulator, the DAP product passes through a rotary
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dryer. After drying, the product is screened to remove oversize and under-
size product. The oversize product is ground in a cage mill and returned
to the granulator along with the undersize fines. The on-size product is
passed through a rotary cooler to storage.
Three separate systems are used to control the particulate,
fluoride, and ammonia emissions from the process. The reactor-granulator
system is equipped with a venturi scrubber followed by a crossflow packed
scrubber of Teller design.
The dryer and cooler are each equipped with separate systems
identical to the reactor-granulator control system, except that in each
case, the venturi scrubber is preceded by a battery of four parallel cyclones
for particulate removal.
Thirty percent acid, diluted to 25% with gypsum pond water, is
used in each venturi scrubber to control fluorides and recover any ammonia
in the gas stream. The spent scrubber liquor is returned to the process.
The packed scrubber serving the reactor-granulator can use either
gypsum pond water containing 1,700 to 1,900 ppm fluoride as F (weight per
volume), or farm runoff water with no fluoride content. The packed
scrubbers serving the cooler and dryer use gypsum pond water as scrubbing
liquor. A total of 130,000 to 150,000 SCFM are discharged from the three
control systems through a common stack.
The first and second set of fluoride and ammonia samples were
collected on 21 March 1973. The process operated at 100-110% of its design
production rate, which is normal. The third and fourth sets of samples were
10
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collected on 22 March 1973. During the first three tests, gypsum pond water
was used in all three packed scrubbers to absorb fluorides. Prior to collec-
tion of the fourth sample, the reactor-granulator scrubber was switched to
using farm runoff water, which is not contaminated with fluorides. The fifth
and final set of samples was collected on 23 March 1973. These samples were
programmed to be collected while the reactor-granulator packed scrubber was
using farm runoff water. Collection of the sample began at 0939. At 0945,
EPA was informed that there was a serious problem with the pump which delivers
farm runoff water to the reactor-granulator scrubber. The scrubber was
switched to using gypsum pond water at about 0948. The scrubbing water was
switched almost instanteously. There was no time when the scrubber was dry
or operating at reduced water flow rates. Sampling was continued without
interruption. Except for this one incident, the process and control systems
were operating at normal and uniform conditions.
The ambient temperature during testing remained around 35°F. At
this temperature, the moisture in the stack gases created a dense plume
which continued for 50-75 ft beyond the stack and rendered visible emission
measurements difficult. However, throughout all five tests runs, there were
visible emissions which remained after the moisture plume dissipated. These
emissions were estimated to be from 10-15% opacity.
IV. LOCATION OF SAMPLING PORTS
Figure 1 shows the location of the sampling ports in the North DAP
stack at ARCO Chemical Company. There are four ports installed 90 degrees
11
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EL. 646'-8-l/2"
BARREL BACK
LADDER
\
GRANULATION BLDG.
ROOF
EL. 616'-6"
INLET
EL. 55T-8-1/2"
<§
©
45<
10'-0-1/2"DIA. (O.D.)
STACK
Figure 1 - DAP Plant Effluent Stack and Platform
12
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apart at 8-1/2 pipe diameters from the upstream disturbance and 2-1/2 pipe
diameters from the outlet. The fluoride samples were taken from three points
in each port at distances of 5-1/4 in., 17-5/8 in., and 35-3/8 in., from the
inside wall at each port.
The Orsat readings were obtained from integrated 30 min gas samples
taken at a distance of 24 in. from the inside wall. The ammonia sampling was
conducted at Point No. 3, Port No. 4 in the stack. Runs were of 1-hr duration.
During the fluoride emission tests, samples of scrubber feed, pond
water makeup, scrubber outlet, feed acid and product, were taken. Figure 2
is a schematic, showing the location of the liquid samples taken. The product
sample was obtained from the plant continuous composite sampler.
V. SAMPLING AND ANALYTICAL PROCEDURES
A. Fluorides
For the particulate fluoride sampling, the Research Appliance Company*
Model 2343 "Staksamplr" equipment was used. The sampling train meets the
specification of the Federal Register. 36, 17 August 1971, with one major
change. The filter was installed between the third and last impinger instead
of between the cyclone and first impinger, and No. 41 Whatman filter paper
was used instead of the glass fiber filter. The analytical method used by
the EPA Laboratory was the Spadns Zirconium Lake.—'
* Mention of a specific company or product does not constitute endorsement
by EPA.
I/ APHA-AWWA-WPCF, "Standard Methods for the Examination of Water and
Wastewater," 13th Edition, 1971, pp. 174-176.
13
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PHOSPHORIC ACID
STACK
1
O
Reactor
Granulator
Dryer
(Pr
imary Scrubber) (Secondary Scrubber)
R- G
Scrubber
j°*'
Dryer
Scrubber
R-G
Tail Gas
Scrubber
|J *
Dryer
Tail Gas
Scrubber
r" •' "•
Cooler
f Product to Storaae
Cooler
Scrubber
to
Cooler
Tail Gas
Scrubber
SAMPLE POINT
A
f M
^
V
B,D,F - Primary Scrubber Feed-Composite (Approx. 25% Phosphoric Acid Solution)
H,J,L - Pond Water Make-Up-Composite
C,E,G- Primary Scrubber Outlet Discharge-Composite
I, K,M-.Secondary Scrubber Outlet Discharge-Separate Samples
Figure 2 - Location of Liquid Samples
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The network of sampling points has previously been described. The
number of points on a traverse, sampling time at each point, and the sampling
sequence were worked out in consultation with the EPA Field Officer. Pre-
liminary measurements were made at the stack to determine temperature and
velocity profiles. A moisture was assumed for the first test run, and cal-
culated for the other tests from the moisture collected in the train on the
previous run.
B. Ammonia
The ammonia sampling was conducted using the RAC* Model 2343 "Stak-
samplr" equipment which meets the specification of the Federal Register, 36,
17 August 1971. There was one change: 100 ml of 30 g/liter HoSO/ was used
in the first two impingers instead of 100 ml of water. The EPA laboratory
used the Kjeldahl Distillation Analytical Method for ammonia.
C. Integrated Gas Samples
The equipment and procedure used for the collection of a cumulative
or integrated gas sample are essentially the same as specified in the Federal
Register. The gas sampling train, which deviates from the train design that
is specified in the Register, is shown in Figure 3. This train design was
approved by EPA prior to the test. The rate of sampling was controlled by
adjusting a micrometer valve which acted as a critical orifice. The sampling
* Mention of a specific company or product does not constitute endorsement
by EPA.
15
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RATE METER
SAMPLE
INTAKE
0\
FILTER
1
AI
C(
PROBE ^
R-COOLED
DNDENSER
N.»-
•^
VALVE
1
TEDLAR
BAG
VACUUM
GAUGE
PURGE LINE
VALVE
-M-
FLOW
CONTROL
VALVE
VACUUM
PUMP
RIGID
AIR-TIGHT
CONTAINER
Figure 3 - Integrated Gas Sampling Train
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rate was set at a constant value for any testing period, such that a total
volume of gases between 1 and 1.5 cu ft were collected.
Analyses for carbon dioxide, oxygen, and carbon monoxide were
performed in the field within a few hours after the sampling was completed,
using an Orsat apparatus.
17
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APPENDIX A
FLUORIDE RESULTS
This appendix contains Tables A-I through A-III. Table A-I shows
the fluoride emission data for the total catch and cyclone catch. Table A-II
is the sample calculations for fluoride total catch and cyclone catch.
Table A-III contains the fluoride data and calculated values for the total
catch and the cyclone catch.
18
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TABLE A-I
FLUORIDE EMISSION DATA
NAME
DESCRIPTION
DOTE OF KU».
ON PROBE TIP OIAMETER
TT NET TIMt: OF HUN
PB BAROMETRIC PRESSURE
PM AVG ORIFICE PRES DROP
VM VOL DRY GAS-METER COND
TM AVG GAS NETER TEMP
VMSTD VOL DPY GAS-STO COND
VW TOTAL H20 COLLECTED
VWV VOL H20 VAPOR-STD COND
PMOS PERCENT MOISTURE rtY VOL
MD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL , DRY
P02 PERCENT 02 8Y VOL, ORY
PCO PERCENT CO RY VOL, DRY
PN2 PERCENT N2 BY VOL, DRY
MWD MOLECULAR wT-DRY STK GA
MW MOLECULAR WT-STK GAS
CP PITOT TUBE COEFFICIENT
DPS AVG STK VELOCITY HEAD
TS AVG STACK TEMPERATURE
NP NET SAMPLING POINTS
PST STATIC PRtS OF STACK
PS STACK PRESSURE, ABSOLUTE
VS AVG STACK GAS VELOCITY
AS STACK AREA
OS STK FLOwRATE, DPY,STD C
OA ACTUAL STACK FLOWRATE
PERI PERCENT ISOKINETIC
B ANISO CORRECTION FACTOR
MF FLUORIDE WT-CYCLONE
MT FLUORIDE WT-TOTAL
1C PERC IMPINGER CATCH
CAN FL. LOAD-PTL,STD CN
CAO FL. LOAD-TTL.STD CN
CAT FL. LOAD-PTL.STK CN
CAU FL. LOAD-TIL, STK CN
CAW FLUORIDE EMIS-PARTIAL
CAX FLUORIDE EMI S- TOTAL
PROCESS FEED RATE
EMISSIONS CYCLONE
EMISSIONS TOTAL
UNITS
IN
WIN
IN.HG
IN.HPO
DCF
DEG.F
DSCF
ML
SCF
S
IN.H20
DEG.F
IN.HG
E IN.HG
FPM
IN2
N DSCFM
ACFM
MG
MG
GR/DSCF
GR/DSCF
GR/ACF
GR/ACF
LB/rlR
LB/rlR
TON P205/HR
LB F/TON P205
LB F/TON P205
IF
03-21-73
.250
120.0
29.80
.914
61. SI
60.3
62.53
91.3
4.33
6.5
.935
.3
20.5
0.0
79.2
28.86
28.16
.850
.320
112.0
24
.02
29.82
1991
11310
135060
156408
88.6
1.000
.50
1.70
71.4
.00012
.00042
.00011
.00036
.14
.49
14.0
.01
.035
2F
03-21-73
.250
120.0
29.78
1.194
72.86
66.4
73.21
109.9
5.21
6.6
.934
.6
21.0
0.0
78.4
28.94
28.21
.850
.353
111.9
24
.03
29.81
2106
11310
142550
165428
98.3
1.000
.70
3.30
78.8
.00015
.00070
.00013
.00060
.18
.85
15.3
.0117
.0555
3F
03-22-73
.250
120.0
29.72
1.101
68.86
60.1
69. 88
102.4
4.85
6.5
.935
.2
20.2
0.0
. 79.6
28.84
28.13
.850
.300
114.3
24
.03
29.75
1923
11310
129498
151009
103.2
1.000
.10
1.90
95.7
.00002
.00042
.00002
.00036
.02
.47
. 18.2
.001
.0258
4F
03-22-73
.250
120.0
29.60
1.194
72.45
61.6
73.03
87.9
4.17
5.4
.946
.4
20.6
0.0
79.0
28.89
28.30
.850
.330
107.3
24
-.03
29.57
2020
11310
138549
158642
100.9
1.000
.80
2.28
64.9
.00017
.00048
.00015
.00042
.20
.57
16.2
.0123
.0351
5F
03-23-73
.250
120.0
29.80
.897
63.30
63.6
63.94
109.1
5.17
7.5
.925
.2
20.6
0.0
79.2
28.86
28.04
.850
.247
110.7
24
.03
29.83
1728
11310
116248
135750
105.3
1.000
0.0
1.60
100
0.0
.00039
0.0
.00033
0.0
.39
14.6
0.0
.0267
-------
TABLE A-II
EXAMPLE FLUORIDE CALCULATIONS
1. VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
17.71*VM*(P8 + PM/13.6)
. ._... VMSTD = .
TM+460.
17.71* 61.51*(29.80+ .914/13.6)
— -- = = 62.53 DSCF
60.3+460.
-2-.— VOLUME OF WATER VAPOR AT STANDARD CONDITIONS
VWV = 0.0474*VW = 0.0474* 91.3 = 4.33 SCF
-3.--PERCENT MOISTURE IN STACK GAS .
100.*VWV 100.* 4.33
PMOS .= = = . 6.5 PERCENT
VMSTD+VWV 62.53+ 4.33
_4......MOLE .FRACTION OF DRY STACK GAS __ '.
100.-PMOS 100.- 6.5
MD = = — = .935 .
100. 100.
-5..__AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS _. . ..._.. . .
MWD = (PC02 * 44/100) + (P02 * 32/100) . . __.
+(PN2+PCO * 28/100)
= ( .3 * 44/100) + (20.5 * 32/100)
_ +(79.2 * 28/100) . _...._.„
= 28.86
..6...-MOLECULAR WEIGHT OF STACK GAS . '.
MW = MWD*MD + 18*<1-MD)
= 28.9* .935 + 18*(1- .935) = 28.16
20
-------
TABLE A-II (Continued)
EXAMPLE FLUORIDE CALCULATIONS
...7. STACK GAS VELOCITY AT STACK CONDITIONS
VS = 4360* SQRT(DPS* (TS+460)) *
...... . . SQHT(1/(PS*MW) ) .
= 4360* SQRT( .320*( 112.0+460))
*SQRT(l/(29.82* 28.16)) = 1991 PPM
-8.--STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS* DRY BASIS
0.123*VS*AS*MD*PS
-OS .... =
TS+460
0.123* 1991* 11310* .935*29.82
• "• •• •» ^ ^ ^ «• •• ^ ^ •» ^ *• •• •• •• •» •• ^ •• ^ •• MV •• •• ^ «• •• ^ <^ ^
112.0 +460
135060 DSCFM
9. STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
QS * (TS + 460) . —- .. _
QA =
17.71 * PS * MD
135060*( 112.0 + 460) . . _.. . .
= 156408 ACFM
17.71*29.82* ..935 - ... - ..—
10. PERCENT ISOKINET1C AND ANISO CORRECTION FACTOR
1032*(TS + 460) *VMSTD
PERI =
... VS*TT*PS*HD*(DN*DN)
1032*( 112.0+460)* 62.53
- 88.6 PERCENT
1991* 120.0*29.82* .935* .250
* .250
1.000
21
-------
TABLE A-II (Continued)
EXAMPLE FLUORIDE CALCULATIONS
11. FLUORIDE LOADING -- PROBE, CYCLONE, AND FILTER
(AT STANDARD CONDITIONS)
CAN = 0.0154 * (MF/VMSTD) * B
-.- - = 0.0154M .50/ 62.53)*!.000
12. FLUORIDE LOADING -- TOTAL (AT
STANDARD CONDITIONS)
CAO = 0.0154 « (MT/VMSTD) * B
= 0.0154M 1.70/ 62.53)*!.000
.00012 GR/DSCF
.00042 GR/DSCF
13. FLUORIDE LOADING -- PROBE, CYCLONE, AND FILTER
(AT STACK CONDITIONS)
__..CAT
17.71*CAN*PS*MD
> ^ •» •«• m ^ mm •» mm, •» •• mm ^ •• <•• MB ••
TS+460
17.71* .0001*29.82* .935
112.0+460
14. FLUORIDE LOADING — TOTAL (AT
.STACK CONDITIONS)
CAU
17.71*CAO*PS*MD
TS+460
17.71* .0004*29.82* .935
: —____ — __-. — ________________.
._ 112.0 + 460 . ... .:.
.00011 GR/ACF
.00036 GR/ACF
22
-------
TABLE A-II (Concluded)
EXAMPLE FLUORIDE CALCULATIONS
15. FLUORIDE EMISSION RATE
— PROBE* CYCLONE, AND FILTER
CAW = 0.00857*CAN*GS
= 0.00857* .0001* 135060
.14 LB/HR
16. FLUORIDE EMISSION RATE'
— TOTAL
CAX = 0.00857*CAO»QS
• = 0.00857* .0004* 135060
.49 LB/HR
23
-------
TABLE A-III
FLUORIDE DATA AND CALCULATED VALUES
RUN-
1F
DATE- 03-21-73
NJ
ATMOS
.TEMP
:DG.F>
43.0
CYCLONE
PORT-
POINT
1 1
_ 1-1
1 2
1 2
1 3
_..! - 3
2 1
... 2 3
2 2
- 2 2
2 3
-2 3.
3 1
-3 1
3 2
-32
3 3
3 3
4 1
- 4 1
4 2
4 2
4 3
4 3
ATMOS
PRES
(I.HG)
29.80
CATCH
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
. 5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20
-.29
METER
VOL
(DCF)
7.50
9.77
11.54
13.38
15.82
18.41
20.81
23.26
25.69
28.14
29.56
30.85
33.55
36.36
39.33
42.42
45.55
48.81
51.50
54.28
57.36
60.55
63.63
66.82
H20
COND •
) (ML)
91.3
DELTA
P
(I.H20)
.240
.240
.240
.200
.200
.300
.300
.260
.260
.260
.070
.070
.390
.390
.450
.460
.450
.490
.350
.410
.410
.f 10
.410
.420
FLUORIDE FLUORIDE
WT-SOL WT-TTL
(MG)
1.70
.50
DELTA
H
(I.H20)
.660
.660
.660
.520
.570
.850
.850
.740
.740
.740
.210
.210
1.100
1.100
1.280
1.300
T.280
1.390
1.000
1.200
1.200
1.200
1.200
1.280
(MG)
1
TEMP
IN
(D.F)
50.0
54.0
55.0
57.0
59.0
61.0
55.0
62.0
65.0
68.0
56.0
58.0
60.0
63.0
67.0
69.0
72.0
74.0
60.0
65.0
71.0
72.0
74.0
74.0
.70
.50
TEMP
OUT
(D.F)
49.0
50.0
50.0
-53.0
54.0
55.0
55.0
56.0
57.0
58.0
58.0
59.0
57.0
58.0
58.0
59.0
60.0
61.0
59.0
60.0
60.0
62.0
62.0
63.0
STACK INIT
AREA VOL
(FT2)
78.54
TRAIN
VAC
(I.HG)
5.0
3.0
3.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
3.0
3.0
6.0
6.5
7.5
7.0
8.0
8.0
6.5
7.0
8.0
8.0
8.0
8.0
(DCF)
5.31
STACK
TEMP
(D;F)
105.0
105.0
105.0
107.0
106.0
107.0
107.0
107.0
108.0
108.0
108.0
109.0
115.0
115.0
120.0
120.0
118.0
118.0
112.0
111.0
112.0
112.0
119.0
115.0
PERC PERC PERC PJTOT
02 C02 CO TUBE
DRY DRY DRY COEF
20.5 .3 0.0 .850
BOX PHOBE
TEMP T DIA VEL
(D.F) (IN) (FPM)
75.0
65.0
65.0
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
1751.3
1751.3
1751.3
1601.6
1600.1
1961.5
1961.5
1826.1
1827.7
1827.7
''948.3
949.2
2252.2
2252.2
2429.7
2456.6
2425.5
2531.0
2128.0
2301.2
2303.2
2303.2
2317.2
2337.2
-------
TABLE _A-III (Continued)
FLUORIDE DATA AND CALCULATED VALUES
N>
ATMOS
--TEMP
(DG.F)
50.0
CYCLONE
PORT-
POINT
1 1
... 1 1
1 2
1 2
1 3
...1 3
2 1
- 2 . 1
2 2
— 2 2
. 2 3
... 2 3
3 1
-.3 1
3 2
3 2
3 3
-3 .3
4 1
. . 4 1
4 2
. 4 2
4 3
_43
ATMOS
PRES
(I.HG)
29.78
CATCH
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20
-.35
METEH
VOL
(DCF)
69.65
72.46
75.34
78.56
81.30
84.12
86.85
89.75
92.46
95.24
97.30
98.99
102.28
105.70
109.20
112.80
116.34
119.92
123.15
126.36
129.74
133.12
136.45
139.74
RUN- 2F DATE- 03-21-73 r,
H20 FLUORIDE FLUORIDE STACK INIT
COND WT-SOL WT-TTL AREA VOL
) (ML)
109.9
DELTA
P
(I.H20)
.350
.350
.380
.410
.330
... .330
.280
.320
.270
.270
.090
.090
.405
.405
.460
.460
.480
.480
.350
.350
.410
.410
.400
.400
(MG)
3.30
.70
DELTA
H
(I.H20)
1.020
1.020
1.120
1.220
1.000
1.000
.970
1.060
.950
.950
.320
. .320
1.450
1.450
1.600
1.600
1.700
1.700
1.250
1.250
1.450
1.450
1.400
1.400
(MG)
3
TEMP
IN
(D.F)
54.0
59.0
67.0
72.0
75.0
76.0
67.0
70.0
76.0
78.0
76.0
74.0
65.0
70.0
76.0
80.0
80.0
81.0
67.0
70.0
71.0
72.0
72.0
70.0
.30
.70
TEMP
OUT
(D.F)
53.0
54.0
55.0
57.0
59.0
61.0
62.0
63.0
64.0
64.0
66.0
66.0
65.0
64.0
64.0
65.0
66.0
66.0
44.0
63.0
63.0
63.0
62.0
62.0
(FT2) <
78.54
TRAIN
VAC
(I.HG)-
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
2.0
2.0
5.0
5.5
6.0
6.0
6.0
6.0
5.0
5.0
5.5
6.0
5.5
5.5
IDCF)
66.88
STACK
TEMP
(D.F)
110.0
110.0
109.0
109.0
120.0
120.0
125.0
125.0
125.0
125.0
122.0
122.0
120.0
110.0
109.0
109.0
109.0
108.0
109.0
105.0
101.0
100.0
100.0
100.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY
21.0 .6
BOX PROBE
TEMP T DIA
(D.F) (IN)
.250
.250
.250
82.0 .250
.250
.250
.250
95.0 .250
.250
.250
.250
.250
69.0 .250
.250
.250
61.0 .250
.250
.250
.250
.250
55.0 .250
.250
.250
.250
DRY
0.0
COEF
.850
VEL
(FPM)
2122
2122
2210
2295
2079
2079
1923
2056
1889
1889
1087
1087
2303
2283
2431
2431
2483
2481
2121
2113
2279
2277
2249
2249
.9
.9
.1
.7
.4
.4
.6
.4
.0
.0
.8
.8
.6
.7
.6
.6
.9
.8
.1
.6
.5
.5
.5
.5 ...
-------
TABLE A-III (Continued)
FLUORIDE DATA AND CALCULATED VALUES
S3
ATMOS
-TEMP -
(DG
45
.F)
.0
CYCLONE
PORT-
-PO
1
_.. 1
1
_ 1
1
— 1
2
2
2
2
2
— 2
3
3
3
— 3
3
.__. 3
4
4
4
4
4
.— 4
INT
1
1
2
2
3
3
1
1
2
2
3
. 3
1
1
2
2
3
3
1
1
2
2
3
3
ATMOS
PRES
(I.HG)
29.72
CATCH
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20
-.35
METER
VOL
(DCF)
142.98
145.40
148.20
151.08
153.78
156.48
159.03
161.58
163.86
166.22
167.48
166.45
171.79
174.93
178.35
181.81
185.31
188.97
192.20
195.45
198.80
202.17
205.57
208.98
RUN- 3F
H20 FLUORIDE
COND WT-SOL
) (ML)
102.4
DELTA
P
(I.H20)
.230
.230
.290
.310
.250
.260
.240
.230
.190
.200
.030
.030
.360
.360
.410
.410
.450
.450
.340
.340
.390
.400
.400
.410
(MG)
1.90
.10
DELTA
H
(I.H20)"
.750
.750
1.020
1.110
.910
.920
.870
.800
.660
.690
.100
.100
1.350
1.350
1.570
1.570
1.700
1.700
1.250
1.250
1.450
1.500
1.500
1.550
DATE- 03-22-73
FLUORIDE STACK
WT-TTL AREA
(MG)
1
TEMP
IN
(D.F)
48.0
54.0
55.0
59.0
58.0
60.0
50.0
56.0
60.0
62.0
61.0
60.0
57.0
65.0
71.0
74.0
77.0
79.0
60.0
68.0
70.0
72.0
75.0
76.0
.90
.10
TEMP
OUT
(D.F)
48.0
50.0
50.0
51.0
52.0
52.0
52.0
52.0
53.0
54.0
55.0
56.0
56.0
57.0
59.0
60.0
62.0
62.0
62.0
62.0
62.0
62.0
63.0
64.0
(FT2)
78.54
TRAIN
VAC
(I.HG)
5.0
5.0
6.0
7.0
6.0
- 6.0
5.0
5.0
4.0
4.0
2.0
2.0
8.0
8.0
8.0
8.5
10.0
10.0
8.5
9.0
9.0
9.0
9.5
9.5
INIT
VOL
(DCF)
140.12
STACK
TEMP
(D.F)
109.0
110.0
110.0
108.0
109.0
108.0
106.0
106.0
108.0
110.0
114.0
113.0
115.0
116.0
116.0
115.0
117.0
115.0
125.0
120.0
118.0
119.0
121.0
122.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY
20.2 .2
BOX PROBE
TEMP T DIA
(D.F) (IN)
.250
50.0 .250
.250
.250
.250
.250
.250
.250
.250
.250
.250
50.0 .250
.250
50.0 .250
.250
.250
.250
.250
50.0 .250
.250
.250
.250
50.0 .250
.250
DRY COEF
0.0 .650
VEL
(FPM)
1723.4
1724.9 -
1936.9
1999.1
1796.8
1830.8 -
1755.9
1718.9
1565.0
1608.5
625.2
624.6
2167.5
2169.4
2315.1
2313.1
2427.6
2423.3
2124.7
2115.6
2261.9
2292.7
2296.6
2327.2
-------
TABLE A-III (Continued)
FLUORIDE DATA AND CALCULATED VALUES
S3
vj
ATMOS ATMOS
-TEMP PRES
(DG.F) (I.HG)
54.0 29.60
CYCLONE CATCH
PORT-
--POINT
1
. 1
1
.. .!_
1
1 .
2
_ 2
2
.... 2
2
_.. 2
3
_ 3
3
. 3
3
3
4
4
4
= . 4
4
4
1
1
2
2.
3
- 3
1
- 1
2
2
3
3
1
1
2
2
3
3
1
1
2
2
3
3
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20
.35
METER
VOL
(DCF)
211.82
214.64
217.92
221.24
224.39
227.50
230.58
233.68
236.23
238.72
240.22
241.49
244.62
247.77
251.13
254.53
258.01
261.54
264.75
267.96
271.31
274.71
278.11
281.54
RUN- 4F DATE- 03-22-73
H20 FLUORIDE FLUORIDE STACK INIT
COND WT-SOL WT-TTL AREA VOL
) (ML) (MG) (MG)
-------
TABLE A-III (Concluded)
FLUORIDE DATA AND CALCULATED VALUES
RUN-
5F
DATE- 03-23-73
00
ATMOS ATMOS
TEMP PRES
(DG.F) (I.HG)
52.0 29.80
CYCLONE CATCH
PORT- SAMP
— POINT TIME
1
- 1
1
1
1
1 .
2
2
2
__. 2
2
2.
3
_. 3
3
... 3
3
_. - 3
4
. 4
4
4
4
_. 4
1
1
2
2
3
3.
1
1
2
2
3
3
1
1
2
2
3
3
1
1
2
2
3
3
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
.5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
-.39
METER
VOL
H20
.COND
(ML)
109.1
DELTA
P
(DCF) (I.H20) I
283.94
286.32
289.03
291.80
294.41
297.03
299.50
302.00
304.24
306.44
307.73
308.83
311.64
314.48
317.55
320.65
323.71
326.80
329.91
332.87
335.90
338.95
341.95
344.95
.190
.190
.260
.270
.230
. .220
.210
.210
.150
.150
.010
.010
.280
.280
.340
.330
.360
.360
.290
.290
.330
.330
.330
.320
FLUORIDE FLUORIDE STACK
WT-SOL . WT-TTL AREA
(MG) (MG) (FT2)
1.60 1.60 78.54
0.0 0.0
DELTA TEMP TEMP TRAIN
H IN OUT VAC
(I.H20)
.685
.685
.930
.960
.830
. .780
.750
.750
.570
.570
.110
.110
1.000
1.000
1.210
1.180
1.300
.1.300
1.050
1.050
1.200
1.200
1.180
1.120
(D.F)
53.0
56.0
60.0
61.0
64.0
64.0
58.0
61.0
64.0
66.0
63.0
63.0
62.0
68.0
70.0
72.0
76.0
76.0
64.0
68.0
72.0
72.0
73.0
73.0
(D.F)
54.0
54.0
55.0
56.0
57.0
58.0
58.0
59.0
60.0
60.0
61.0
62.0
62.0
63.0
64.0
65.0
66.0
67.0
65.0
65.0
65.0
66.0
66.0
66.0
(I.HG)
4.0
5.0
5.0
5.0
5.2
... 5.5
5.0
5.0
4.0
4.0
2.0
2.0
6.0
6.0
7.0
7.0
8.0
8.0
7.0
7.0
8.0
8.0
7.0
7.0
INIT PERC PERC PERC PITOT
VOL 02 C02 CO TUBE
(DCF) DRY DRY DRY COEF
281.65 20.6 .2 0.0 .850
STACK BOX PROBE
TEMP TEMP T DIA VEL
(D.F) (D.F)
109.0
110.0
110.0
109.0
107.0
110.0 • ..
108.0 50.0
110.0
110.0
110.0
110.0
110.0
112.0
112.0
112.0
112.0
112.0
110.0
110.0
112.0
110.0
110.0
115.0 60.0
114.0 60.0
(IN)
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
(FPM)
1566.8
1568.2
1834.4
1867.7
1720.8
1687.4 -
1645.7
1648.6
1393.4
1393.4
359.8
359.8
1907.0
1907.0
2101.4
2070.3
2162.4
2158.6 .
1937.4
1940.8
2066.7
2066.7
2075.7
2042.2
-------
APPENDIX B
GASEOUS RESULTS
Tables B-I, B-II, and B-III contain the results of the testing for
ammonia in the stack gas from the DAP plant. Table B-I contains the summary
of results, and Table B-II contains the ammonia emission data. Table B-III
contains the ammonia data and calculated values.
The results of the moisture and Orsat analysis are presented in
Section III of this report.
29
-------
NAME
OS
-QA
PMOS
-PC02 —
P02
PCO -
AMMONIA
MT
-CAO
CAU
CAX
OUjvlliAivJL
DESCRIPTION
DATE OF RUN
STK FLOWRATE* DRY»STD CN
ACTUAL STACK FLOWRATE
PERCENT MOISTURE BY VOL
PERCENT C02 BY VOL> DRY
PERCENT 02 BY VOL» DRY
PERCENT CO BY VOL» DRY
-- TOTAL CATCH
AMMONIA WT-TOTAL
AMMONIA LOAD-TTL,STD CNi
AMMONIA LOAD-TTL,STK CN
AMMONIA EMI S- TOTAL
TABLE B-I
\J 1. ixuoU.Lj.Lo
UNITS
DSCFM
ACFM
MG
GR/DSCF
GR/ACF
LB/HR
AMMrtMT A
- AMMONIA
1-NH3
03-21-73
149763
170816
7.0
.3
20.5
0.0
< .30
2-NH3 3-NH3 4-NH3
03-21-73 03-21-73 03-22-73 03-23-73
149763
170816
7.0
.3
20.5
0.0
166169
188266
6.7
.6 --
21.0
• - •• 0.0
162765
184013
6.4
.2
20.2
0.0
151092
171879
7.5
.2
20.6
0.0
:< .30
< .30
< .30
DATE OF OUTPUT 07-13-73
.PROGRAM DATE 01-31-72
-------
TABLE B-II
AMMONIA EMISSION DATA
NAME
DN
-TT
PB
PM -
VM
-TM. ._.
VMSTD
-VW
VWV
PMOS ._
MD
PC02..
P02
PCO ..
PN2
MWD.__.
MW
CP
DPS
TS
NP
.PST1__
PS
_VS
AS
OS
QA
.PERI ...
B
DESCRIPTION
DATE OF RUN
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL.
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL» DRY
PERCENT 02 BY VOL» DRY
PERCENT CO BY VOL, DRY
PERCENT N2 BY VOL, DRY
MOLECULAR WT-DRY STK GAS.
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE, DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
ANISO CORRECTION FACTOR
UNITS
IN
MIN
IN.HG
IN.H20
DCF
DEG.F
DSCF
ML
SCF
. -_ ._ .
IN.H20
DEG.F.
IN.HG .
IN.HG
•FPM .
IN2
DSCFM
ACFM
1-NH3
03-21-73
.250
60.0
29.80
- 1.844
43.79
62.1
44.46
70.5
3.34
7.0
.930
. .3
20.5
0.0
79.2
28.86
28.10
... . .850
.372
. 99.8
12
. -0.00
29.80
2175
11310
149763
170816
113.6
1.000
2-NH3
03-21-73
.250
60.0
29.87
-. - 1.845
43.67
73.0
43.54
65.7
3.11
6.7
.933
.6
21.0
0.0
78.4
.._ . 28.94
28.20
.850
.456
99.7
12
.__..... .03.
29.90
2397
11310
. 166169
188266
. . 100.2
1.000
3-NH3
03-22-73
.250
60.0
29.72
1.840
44.93
62.5
45.46
65.8
3.12
6.4
.936
.2
20.2
0.0
79.6
- .... 28.84
28.14
.850
.434
97.3
12
.03
29.75
2343
11310
.162765
184013
106.3
1.000
4-NH3
03-23-73
.250
60.0
29.. 80
1.840
42.68
65.3
43.08
73.2
3.47
7.5
.925
.2
20.6
0.0
79.2
. . 28.86
28.05
.850
.382
96.0
12
.03
29.83
2188
11310
151092
171879
109.0
1.000
-------
TABLE B-III
AMMONIA DATA AND CALCULATED VALUEg
RUN- 1-NH3 DATE- 03-21-73
ro
ATMOS
.TEMP
DG.F)
43.0
PORT-
POINT-
..
. .. _
,
ATMOS STACK
PRES VAC
(I.HG) (I.H20)
29.80 0.00
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
. 5.00
METER
."•" VOL
(DCF) (
939.54
943.35
947.30
951.06
954.03
958.38
961.09
965.51
969.41
972.72
976.26
979.84
H20
COND
(ML)
70.5
DELTA
P
I.H20)
.365
.370
.360
.370
.375
.380
.370
.370
.370
.380
.380
.380
PARTIC PARTIC STACK INIT
WT-PTL WT-TTL AREA VOL
(MG) (MG) (FT2) (DCF)
< .30 <
DELTA
H
(I.H20)
1.840
1.840
1.840
1.840
1.840
1.850
1.850
1.840
1.840
1.900
1.850
1.800
TEMP
IN
(D.F)
55.0
58.0
63.0
68.0
70.0
70.0
70.0
71.0
71.0
.72.0
72.0
73.0
.30 78.54 936.05
TEMP
OUT
(D.F)
51.0
51.0
53.0
54.0
56.0
-57.0
57.0
59.0
59.0
60.0
60.0
61.0
TRAIN
VAC
(I.HG)
8.5
8.5
8.0
7.0
7.0
.... 7.0 -
7.0
7.5
8.0
9.0
10.0
13.0
STACK
TEMP
(D.F)
105.0
102.0
100.0
96.0
96.0
95.0
98.0
94.0
100.0
106.0
106.0
101.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY DRY COEF
20.5 .3 0.0 .850
BOX PROBE
TEMP T DIA
(D.F) (IN)
50.0 .250
52.0 .250
.250
.250
.250
- .250
.250
.250
.250
.250
.250
.250
VEL
(FPM)
2162.7
2171.7 -
2138.3
2160.1
2174.6
2187.1-
2163.9
2156.2
2167.8
2206.7
2208.7
2198.9
-------
TABLE B-III (Continued)
AMMONIA DATA AND CALCULATED VALUES
u>
ATMOS ATMOS
-TEMP PRES
(DG.F) (I.
50.0 29
HG)
.87
PORT- SAMP
-POINT TI
(MI
3 1 5.
5 .
.5.
.... 5.
5.
5 .
5.
5.
5.
5 .
5.
„__ 5.
ME
N)
00
00
00
00
00
00
00
00
00
00
00
00
STACK
VAC
(I.H20)
-.35
METER
VOL
(DCF) (I
984.22
987.90 ...
991.39
995.03
998.60
1002.37
1005.95
1009.60
1013.31
1017.02
1020.67
1024.35
RUN- 2-NH3 DATE- 03^21-73
H20 PARTIC PARTIC STACK INIT
COND
(ML)
65.7
DELTA
P
.H20)
.500
.460
.450
.460
.460
.460
.450
.450
.450
.450
.440
.440
WT-PTL
(MG)
< .30
DELTA
H
(I.H20)
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.900
WT-TTL
(MG
< .
TEMP
IN
(D.F) (
57.0
65.0
74.0
80.0
84.0
87.0
88.0
88.0
90.0
93.0
94.0
93.0
)
30
TEMP
OUT
D.F)
54.0
55.0
57.0
60.0
62.0
63.0
66.0
66.0
67.0
68.0
70.0
70.0
AREA
(FT2)
78.54
TRAIN
VAC
(I.HG
5.0
5.0
5.5
- 6.0
6.0
6.0
6.5
7.0
7.0
7.5
8.0
10.0
VOL
(DCF)
980.68
STACK
TEMP
) (D.F)
98.0
98.0
99.0
99.0
100.0
100.0
100.0
100.0
100.0
101.0
101.0
101.0
PERC PERC PERC P
02 C02
DRY DRY
21.0 .6
BOX PROBE
TEMP T DIA
(D.F) (IN)
.250
.250
50.0 .250
50.0 .250
.250
.250
.250
.250
.250
.250
.250
. .250
CO
DRY
0.0
ITOT
TUBE
COEF
.850
VEL
(FPM)
2507
2404
2380
2406
2408
2408
2382
2382
2382
2384
2358
2358
.0
.6
.4
.7
.9
.9 -
.6
.6 -
.6
.7
.0
.0
-------
TABLE B-III (Continued)
AMMONIA DATA AND CALCULATED VALUES
' . . . . . RUN- 3-NH3 DATE- 03^22-73 . ...
ATMOS ATMOS
TEMP. „ PRES
(DG.F) (I.
45.0 29
HG)
.72
PORT- SAMP
POINT. TI
(MI
3 1 5.
. 5.
5.
5.
5.
5 .
5.
.. 5.
5.
5.
5.
5.
ME
N)
00
00
00
00
00
00
00
00
00
00
00
00
STACK
VAC
(I.H20)
-.35
METER
VOL
(DCF) (
28.55
32.19
35.85
39.58
43.35
47.10
50.80
54.57
58.32
62.09
65.89
69.73
H20
COND
(ML)
65.8
DELTA
P
I.H20)
.430
.430
.430
.430
.430
.430.
.430
.430
.440
.440
.440
.450
PARTIC
WT-PTL
(MG)
<.30
DELTA
H
(I.H20)
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
PARTIC
WT-TTL
(MG)
<
TEMP
IN
(D.F)
50.0
60.0
66.0
69.0
72.0
73.0
75.0
76.0
76.0
76.0
78.0
78.0
.30
TEMP
OUT
(D.F)
45.0
48.0
50.6
52.0
53.0
55.0
56.0
57.0
58.0
56.0
60.0
60.0
STACK INIT PERC PERC PERC PITOT
AREA VOL 02 C02 CO . TUBE •__
(FT2)
78.54
TRAIN
VAC
(I.HG)
8.0
8.0
9.0
9.0
9.0
9.0
9.0
9.0
9.0
9.5
10.0
10.5
(DCF) DRY
24.80 20.2
STACK BOX
TEMP TEMP
(D.F) (D.F)
97.0
97.0 .
97.0
. 98.0
95.0
95.0 50.0
95.0
95.0
100.0
101.0
99.0
98.0
DRY
.2
PROBE
T DIA
(IN)
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
DRY COEF
0.0 .
VEL
(FPM
2331.
2331.
2331.
2333.
2327.
2327.
2327.
2327.
2364.
2366.
2362.
2386.
850
... ._ ....
>
2
2 . .. .
2
3 -
0
0
0
0
5
6
4
9
-------
TABLE B-III (Concluded)
AMMONIA DATA AND CALCULATED VALUES
RUN- 4-NH3 DATE- 03-23-73
ATMOS ATMOS STACK H20
...TEMP PRES VAC COND
(DG.F) (I.HG) (I.H20) (ML)
52.0
29.80
-.35
73.2
PARTIC
WT-PTL
(MG)
< .30
PARTIC STACK INIT PERC PERC PERC PITOT
WT-TTL AREA VOL 02 C02 CO TUBE
(MG) (FT2) (DCF) DRY DRY DRY COEF
< .30 78.54 69.81 20.6 .2 0.0
,850
Ul
PORT- SAMP
POINT TIME
(MIN)
4 5.00
_ . - 5.00
5.00
— - 5.00
5.00
— — 5.00
5.00
5.00
5.00
. . 5.00
5.00
„-_ i. 5.00
METER
VOL
(DCF)
73.24
76.88
80.34
83.86
87.41
91.00
94.54
98.09
101.70
105.27
108.86
112.49
DELTA
P
(I.H20)
.380
.380
.380
.375
.375
.260
.290
.325
.405
.420
.480
. .520
DELTA
H
(I.H20)
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
1.840
TEMP
IN
(D.F)
61.0
66.0
68.0
70.0
71.0
73.0
73.0
73.0
74.0
74.0
76.0
76.0
TEMP
OUT
(D.F)
54.0
55.0
56.0
57.0
58.0
60.0
60.0
61.0
62.0
62.0
63.0
64.0
TRAIN
VAC
(I.HG)
8.0
7.7
7.7
7.7
8.0
8.0
8.0
8.0
8.0
8.0
9.0
9.0
STACK
TEMP
(D.F)
100.0
100.0
98.0
97.0
96.0
95.0
95.0
94.0
94.0
95.0
94.0
94.0
BOX PROBE
TEMP T DIA VEL
D.F) (IN) (FPM)
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
2198
2198
2194
2177
2175
1810
1911
2022
2257
2300
2457
2557
.2
.2 .
.3
.8
.9
.2
.7
.0
.2
.7.
.3
.6
-------
APPENDIX C
OPERATIONS RESULTS
The production rates of the ARCO Chemical Company Diammonium
Phosphate Plant at Fort Madison, Iowa, during the week we tested, are
contained in Table C-I. During the first testing day, the process
operated at 100-110% of design rate which is considered normal for
this plant.
36
-------
Date
21 March 1973
21 March 1973
22 March 1973
22 March 1973
22 March 1973
TABLE C-I
PRODUCTION RATE
Run No.
1
2
3
4
5
Tons P205/Hr
14.0
15.3
18.2
16.2
14.6
37
-------
APPENDIX D
FIELD DATA
This section presents the actual field data from the testing.
38
-------
MIDWEST RESEARCH INSTITUTE
RUN
MRI Project Number 3S13S'- &
Field Dotes '3 - )<| , - 3.. g y: -
Plant A-#£O 0
Sampling Location
Crew Chief .^) ^,
-------
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
PLANT _
DATE
SAMPLING LOCATION
INSIDE OF FAR WALL TO
OUTSIDE OF NIPPLE, (DISTANCE A)
INSIDE OF NEAR WALL TO
OUTSIDE OF NIPPLE, (DISTANCE B) _
STACK I.D.. (DISTANCE A - DISTANCE B)
NEAREST UPSTREAM DISTURBANCE
NEAREST DOWNSTREAM DISTURBANCE.
CALCULATOR.
SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
/
^
3
FRACTION
OF STACK I.D.
4<^
A// 7
>?,.§-
STACK I.D.
/>£>
/(
1 1
PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1/8 INCH)
6~fa
j~?s/£
3$3/zr
DISTANCE B
ic'/Z
tt
l i
TRAVERSE POINT LOCATION
FROM OUTSIDE OF NIPPLE
(SUM OF COLUMNS 4 & 5)
s.^"
a.% '/?
4$y&
EPA (Our) 232
4/72
40
-------
PRELIMINARY VELOCITY TRAVERSE
PLANT.
DATE_
4ECO
LOCATION Pr?P
STACK ID. IP
BAROMETRIC PRESSURE, in. Hg.
STACK GAUGE PRESSURE, in. H2Q
OPERATORS
SCHEMATIC OF TRAVERSE POINT LAYOUT
TRAVERSE
POINT
NUMBER
/
^
^
SL//^
/ ]/^
I
•
AVERAGE
VELOCITY
HEAD
(Aps), in.H20
G &
£><(£X
/s^9
Or^^~
&f4h
6,33
STACK
TEMPERATURE
(Ts), °F
v^^
/£>t-L
y ^^
; & )
IT) I
/
-------
r-i
PLANT
DATE 7\
SAMPLING LOCATION
NOMOGRAPH DATA
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg -^^3^'' *•>£>
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
Tmavg.
Bwo
Pm
ps
Ps/pm
savg.
*Pavg.
APmax.
£^
'?tfo&
0??.^
$1,8/3
1-0
/• r< j _ l
w ^^ (*J^^±.
0(4
oAf-
/
' oc
r*j *\
1 VT* *~J
./f /
EPA (Out) 234
4/72
42
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT
DATE
A £ c
COMMENTS:
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION
I
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS)
ANALYTICAL METHOD /O/?,S
AMBIENT TEMPERATURE *f
OPERATOR
^\^^ RUN
GAS ^"^-^
C02
D£ (NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N £ (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING
#
20%
yo. y
NET
^
<
1.0,*
O
2
ACTUAL
READING
^3
>,7
Ml
NET
^
X),$
O
3
ACTUAL
READING
.2
MV
?e-<7
NET
P-
•yo.1
0
AVERAGE
NET
VOLUME
fe<3^£>
••' \
&$-
€>
MULTIPLIER
44/100
I..._JT
32/100
_ ,. 1
^/lOO
^/lOO
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole
TOTAL
EPA (Dui) 230
A/72
-------
FIELD DATA
PLANT 4_
DATE.
\cb .
SAMPLING LOCATION _j) fit
SAMPLE TYPE /-/C-LI'
RUN NUMBER /?
OPERATOR it
AMBIENT TEMPERATURE ' *?
BAROMETRIC PRESSURE "1- ')•
PROBE LENGTH AND TYPE_=
NOZZLE I.D ;.c*£_.v_?
ASSUMED MOISTURE.3,.
SAMPLE BOX NUMBER _
METER BOX NUMBER
METER AHg
C FACTOR. i
STATIC PRESSURE. (P \ Jy
FILTER NUMBER (s) /
SCHEMATIC Of TRAVERSE POINT LAYOUT
PROBE HEATER SETTING!
HEATER BOX SETTING
REFERENCEip i
READ AND RECORD ALL DATA EVERY.
MINUTES
TRAVERSE
POINT
NUMBER
CLOCK TIME
GAS METER READING
(Vml. It3
VELOCITY
HEAD
(APS). in. H20
ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H20)
DESIRED ACTUAL
STACK
TEMPERATURE
(TS).°F
DRY GAS METER
TEMPERATURE
INLET
(Tmin).°F
OUTLET
PUMP
VACUUM.
in. Hg
SAMPLE BOX
TEMPERATURE.
°F
IMPINGER
TEMPERATURE.
il
_£L
7,3'
/42?
4L
no
i /
o,
&-
0,57
3
/O tl
-------
7V
3
l-F
TRAVERSE
POINT
NUMBER
4/-3
\s. CLOCK TIME
$TTrUNG XcScK,
TIME, mm X^
' ' -____
* /?£>.
/4
ACTUAL
(•*r
h^
STACK
TEMPERATURE
(Tsl.°F
//?
//• 5
DRY GAS METER
TEMPERATURE
INLET
'Tm iB).°F
1U
7
-------
ANALYTICAL DATA
PLANT
COMMENTS:
HATF 3-£\ - 73
SAMPLING LOCATION t>Af (/lAA^jM&rts ) ^
SAMPLFTYPE , f-A«-i.oK£e
/ _ \ C
RMNNUMRFR ( / — /~ A £>/?/£>£. ) r""~
SAMPLF BOX NUMBER "^
CLEAN-UP MAN f^-U fJ U It) &>~\{AW
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
vU
MO'STURE (Uc^L
IMPINGERS ' -£ f)
FINAI VOLI1MF •? & «» ml tyt/frM/
INITIAI vnillMF 3. && ml
NFT vni IIMF & C? ml
SILICA GEL / r°i n
FINAI WFIRHT ^ ^ '' ' g g
INITIAL WF'KHT /? •?&.&? % g
NFJ WFir,HT 13 .• / g g
EPA (Dur) 231
4/72 .
LABORATORY RESULTS
CONTAINER me
CONTAINER me
FRONT HALF SUBTOTAL mp
r.nNTAINFR mp
ETHER-CHLOROFORM
FXTRA^TinN mg
CONTAINER mg
BACK HALF SUBTOTAL mE
TOTAI WFIRHT mg
Q
s Svu^cv^MJO /2-^ M^
i/^ -jj/uJ^L ^T^y fl
/ /e^v^* d
-------
FIELD DATA
y
PLANT A f$ C. L/ .
DATE J/J-II13
PROBE LENGTH AND TYPE ** \3 -i^Sl^U;-^
SAMPLING LOCATION $ K C p
SAMPLE TYPE Vl/fS ,
RUN NUMBER ^ AS H 3 ~ /
OPERATOR
x^..«.^>«w
AMBIENT TEMPERATURE ' ff.'3 '
TRAVERSE
POINT
NUMBER
•*$2{
^//
\J-dt -y
*3
BAROMETRIC
STATIC PRE
FILTER NUM
\. CLOCK TIME
TIME, min ^x.
~~7o~57r~^~— __
(i -03 $
lid £> I0
.11(3' /V
i 1 1 5 7«^
f/2-3 £>'
/^ 2? ^
,,^3 £
\l?& *c
{H2 «*
i/Yf? i«
/ /3 3 .'/>'
i(5? <;«>
: PRESSURE A'/-5'
iSURF, (Ps)
RFR (c) / - it>/-/j
NOZZLE I.D
ASSUMED M(
SAMPLE BO
METER BOX
METER iH,
C FACTOR
)ISTURE. 3, _
X NUMBER
/''
3£>Vo
NUMBER £?
* V7 *,'
PROBE HEATER SETTING
HEATER BOX SETTING
3~0
(*f5cf-
REFERENCE «vn / &->
^ SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERJT_^!L_ MINUTES
GAS METER READING
£•? "•? fy i ^J-1^)
onci ffl
VELOCITY
HEAD
(AP-), in. H70
5 c
cr,3(^5'
/*") "^7
C'/.?^
,3 7
, 375
, 3?
.37
i'tf
i"^7
i i»
J?V
^(?
ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H20)
DESIRED
/,&L
i&
i.y+
A$y
j.tf5
[ &5
hi?
if$v
life
l j£
iito
ACTUAL
f
•a.
:
STACK
TEMPERATURE
(TS).°F
L^
i n'Z-*
'/Oft
/'t)
5"«?
-
COMMENTS:
EPA lOuil 235
-------
ANALYTICAL DATA
PLANT.
DATE_
AHC.O
3/3//73
SAMPLING LOCATION *.
SAMPLE TYPE
RUN NUMBER.
//•
SAMPLE BOX NUMBER.
CLEAN-UP MAN.
v.<\ V^ov
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS), CONTAINER.
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER CONTAINER
LABORATORY RESULTS
.nig
.rag
FRONT HALF SUBTOTAL
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
S€>
MOISTURE
IMPINGERS
FINAL VOLUME
INITIAL vm iiHFggO
VOLUME 4&$ &-
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT ^
NET WEIGHT _
EPA (Dur) 231
4^2
CONTAINER
ETHER-CHLOROFORM
CONTAINER.
.mg
BACK HALF SUBTOTAL
mg
WEIGHT
IDE
TOTAL MOISTURE
48
-------
NOMOGRAPH DATA
PLANT frit CO
DATE
SAMPLING LOCATION
jjV?"F
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE IVIETER TEMPERATURE (AMBIENT + 20eF),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER; in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
Tmavg.
Bwo
pm
0,D ft
Ps
Ps/Pm
savg.
*Pavg.
APmax.
\*t
•}b
1%
Wit
tf>1®
1
iH
,31
Jtt
oW
0^
0/>^>
0,**
EPA (Dur) 234
4/72
49
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT.
DATE_
COMMENTS:
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION ~J~)
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS!
ANALYTICAL METHOD
AMBIENT TEMPERATUR
OPERATOR
^^^^ RUN
GAS ^^"\
C02
O£(NET is ACTUAL o2
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N 2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING
7(,l
^
NET
,(•
il,^
D
2
ACTUAL
READING
n<-
37, *
NET
,?
%w
0
3
ACTUAL
READING
n&
y.'d
NET
£
w,z
D
AVERAGE
NET
VOLUME
MULTIPLIER
44/100
i. ^:~
32/100
_ - 1
^/lOO
^/lOO
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole
TOTAL
Ln
O
EPA (Dur) 230
4/72
-------
FIELD DATA
PLANT.
DATE
AX?
/
SAMPLING LOCATION D frP A/,
SAMPLE TYPE F~/<
RUN NUMBER _
OPERATOR
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE .
STATIC PRESSURE. (Ps)_
FILTER NUMBER (s)
PROBE LENGTH AND TY/E.
NOZZLE I.D..
ASSUMED MOISTURE.'.
SAMPLE BOX NUMBER
METER BOX NUMBER _
METER AH
C FACTOR
/ ,
SCHEMATIC OF TRAVERSE POINT LAYOUT
PROBE HEATER SETTING t&TJ
HEATER BOX SETTING.
REFERENCE Ap
READ AND RECORD ALL DATA EVERY.
"**-..
MINUTES
TRAVERSE
POINT
NUMBER
CLOCK TIME
GAS METER READING
VELOCITY
HEAD
(Aps), in. H20
ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H20)
STACK
TEMPERATURE
(TS).°F
DRY GAS METER
TEMPERATURE
INLET OUTLET
PUMP
VACUUM.
in. Hg
SAMPLE BOX
TEMPERATURE.
°F
IMPINGER
TEMPERATURE.
"F
IG/'
r i
V
U-
3EI
. 7
z*.
A
^£
3
4-tfL
/o
10
-70
, 5
5"
/7
103
/o
-U-
A 60
/>6O
yc?
65"
n
/Mo
6/0
VB
to
no
/ y i
9
/D
3
o
0^1
n^L
COMMENTS:
EPA (Dun 235
-------
TRAVERSE
POINT
NUMBER
¥/3
3
\. CLOCK TIME
_____
£ / 8 >•£
/O /%bO
' —
GAS METER READING
'V- "3
/ 3 £> / t-/S~O
1 3*7 /• '~7i-J-D
h f° S^~f
' / y^
*7 ^2—X^/t,
/ -^ *\*>r <_^ /
VELOCITY
HEAD
lilpjl. in. H^O
d ft-/-
O
-------
ANALYTICAL DATA
PLANT
nATF -3
1 - 73
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
P feP/J/U O
SAMPLE BOX NUMBER
CLEAN-UP MAN O U/JAJ/A) 6
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS), CONTAINER
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER CONTAINER
LABORATORY RESULTS
.mg
.mg
FRONT HALF SUBTOTAL
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
MOISTURE
53
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER.
BACK HALF SUBTOTAL
.mg
.mg
.mg
.mg
TOTAL WEIGHT
me
IMPINGERS -, 0.. /
FINAI VOI I1MF f-/fe>/ ml ^
INITIAI VOI (IMF 'ZteKt . ml P
NFTVnillMF ff-5?'&7~ti\ - —
SILICA GEL / A
FINAI WEIGHT CSX- -1 g
INITIAI WEIRHT ^/^Zg
NET WEIGHT )tf fl g
EPA (Dur) 231
4^2
g
g
I
B
B
?:
TOTAL MOISTURE
-------
Ul
TRAVERSE
POINT
NUMBER
JL
j/.
c*
7
il
COMMENTS:
EPA iDutl 235
FIELD DATA
?/w)-)
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
OPERATOR _
AMBIENT TEMPERATURE .
BAROMETRIC PRESSURE .
STATIC PRESSURE, (Ps)_
FILTER NUMBER (s)
PROBE LENGTH AND TYPE
NOZZLE I.D._
ASSUMED MOISTURE.',
SAMPLE BOX NUMBER
METER BOX NUMBER .
METER AHg,_
C FACTOR
/,
PROBE HEATER SETTING.
HEATER BOX SETTING
REFERENCE AP
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY.
MINUTES
CLOCK TIME
/fr-?o
//^
GAS METER READING
-------
ANALYTICAL DATA
PLANT
DATF 3 —
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER L
SAMPLE BOX NUMBER
CLEAN-UP MAN
M. /vxr-j-w <«
/0£..
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS), CONTAINER.
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER CONTAINER
LABORATORY RESULTS
.nig
.mg
FRONT HALF SUBTOTAL
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,.
AND BACK HALF OF FILTER HOLDER
MOISTURE
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
.mg
.mg
.mg
_mg
me.
IMPINGERS ~>
FINAI vm IIMF ^- .-
INITIAL VOLUMES
NET V™ IIMF e#
SILICA GEL -
FINAI WFIfiHT 6*
INITIAL WEIGHT <£:
NFT WFIRHT
EPA (Dur) 231
4/72
*& t^
? & mlc —
DO m|
*•>(*£*.. ml
///„ /)
g g
:5£>'3 g g
Y rt 8 E
B
E
E;
TOTAL MOISTURE
55
-------
r
NOMOGRAPH DATA
DATE.
SAMPLING LOCATION
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in. .
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
T|"avg.
Bwo
pm
.$(3
PS
Ps/pm
savg.
APavg.
APmax.
I. tf)
W
^a
1%
^n^
^, 1%
0&'
!
110
£>'fo
0,4?
a?^
,>s
,>»
h ^
EPA (Dur) 234
4/72
56
-------
ui
7"
FIELD DATA
PLANT.
DATE_
C O
SAMPLING
SAMPLE TYPE
RUN NUMBER.
OPERATOR
g
r f I\J,
t
AMBIENT TEMPERATURE .
BAROMETRIC PRESSURE .
STATIC PRESSURE, (Ps)_
FILTER NUMBER (s)
¥'
PROBE LENGTH AND TYPE
NOZZLE I.D.___£K.._
ASSUMED MOISTURE. ',
SAMPLE BOX NUMBER
METER BOX NUMBER
METER AH@ h •
CFACTOR
Oc
SCHEMATIC OF TRAVERSE POINT UYJ
READ AND RECORD ALL DATA FVFRY 5 MINUTES
T LAYJ1UI-
«-> MINI
PROBE HEATER SETTING
HEATER BOX SETTING.^
REFERENCE Ap
TRAVERSE
POINT
NUMBER
r///
3
CLOCK TIME
F
E, mm
10 / OW
1/0?
///-/
II 3V
/ o 3
h.o"3*
6.3G
o
COMMENTS:
fPA iHuil ?Vi
ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H20)
0, I
LLL
ffl
.17
0,80
0*16
A 35
A 57
1, 5 7
/,70
IP3
ACTUAL
Jf/
0.80
C. /O
o.io
1.37
/. 70
I, 70
STACK
TEMPERATURE
(TS),°F
/l O
//O
'/of
IOC?
//y
t/3
/o
/I*
US
DRY GAS METER
TEMPERATURE
INLET
(Tmjn).°F
JL
•fc
56
Cis
65-
7V
7-
70
OUTLET
57
5" 3
Co
6
PUMP
VACUUM.
in. Hg
eT*
7
/O
8 -
i
0
SAMPLE BOX
TEMPERATURE,
°F
cv
(.C,
gr
cfr
73
75"
7:2-
75
76
IMPINGER
TEMPERATURE,
-------
os
TRAVERSE
POINT
NUMBER
H\-S
\. CLOCK TIME
SA«PUNG\ c^
TIME.min \_
__
5 * ft*
ID J 'lvV>>
-
GAS METER READING
' V- "J
9*0 £,k 7 O
*0%.9 ftSL
VELOCITY
HEAD
(4pji. in. t^O
OfLt°
Q.*tf
ORIFICE PRESSURE
DIFFERENTIAL
IAH). in H20i
DESIRED
h$
/,*
ACTUAL
0
r
STACK
TEMPERATURE
iT$i.°F
/9> /
12?-
DRY GAS METER
TEMPERATURE
INLET
IT,, in'.°F
79
n
OUTLET
'Tmout'.uF
6*3
^
PUMP
VACUUM.
in »l
K 'h
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT.
DATE_
A-.fi.CQ
COMMENTS:
/
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION *Ptt P
fl/ , ST
('<*-
SAMPLE TYPE (BAG, INTEGRATED. CONTINUOUS)
ANALYTICAL METHOD C> tf £? "T~
AMBIENT TEMPERATURE
OPERATOR fcgC L'i'TS i-T)
^\^^ RUN
GAS ^^-^
C02
02 (NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
M£ (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING
V
A 43
W
NET
*'/
zoa
D
2
ACTUAL
READING
D.^
^?.2-
y^
NET
0.2-
lJ®
0
3
ACTUAL
READING
Oi 2—
W •+
3-0. j
NET
t>.2^
yo,2-
d
AVERAGE
NET
VOLUME
A-z-
20* 1^
o
MULTIPLIER
44/100
i. .._::r
32/ioo
_ . 1
a/ioo
a/100
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole
TOTAL
VO
EPA (Our) 230
A/72
-------
ANALYTICAL DATA
PLANT (
DATE 2.
~ 75
SAMPLING LOCATION
SAMPLE TYPE HU.O
RUNNUMBER_
SAMPLE BOX NUMBER
CLEAN-UP MAN
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS), CONTAINER.
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER CONTAINER
LABORATORY RESULTS
.nig
.nig
FRONT HALF SUBTOTAL
.nig
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
MOISTURE
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
.mg
.mg
.mg
_mg
TOTAL WEIGHT
_mg
IMPINGERS
FINAL VOLUME ^
INITIAL VOLUME "^<
SILICA GEL xj
FINAI WFIfiHT &0
INITIAL WEIGHT <£=^
NFT WFIGHT /
EPA (Dur) 231
4/72
i¥
' /ml ^
f!?O ml /},
^7 ml ^/
-------
FIELD DATA
PLANT
DATE.
SAMPLING LOCATION fift? £
SAMPLE TYPE A//-J 3
RUN NUMBER ^
OPERATOR .S
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE, (P.J
FILTER NUMBER (s)
'-L
SCHEMATIC OF TRAVERSE POINT LAYC
READ AND RECORD ALL DATA EVERY.
'OINT LAYOUT
1 5 Ml
PROBE LENGTH AND TYPF . 6> (a / •
NOZZLE I.D.. UM* - —X. -
ASSUMED MOISTURE. ', "7 "^
SAMPLE BOX NUMBER
METER BOX NUMBER .
METER AHg
C FACTOR
PROBE HEATER SETTING.
HEATER BOX SETTING
REFERENCE ip
MINUTES
COMMENTS:
EPA (Dull 235
-------
ANALYTICAL DATA
PLANT.
HATE ~
SAMPLING LOCATION
SAMPLE TYPE __4-
RUNNUMBER_
SAMPLE BOX NUMBER
CLEAN-UP
AJ
COMMENTS:
•J
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
CONTAINER.
CONTAINER
LABORATORY RESULTS
mg
.nig
FRONT HALF SUBTOTAL
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
BACK HALF SUBTOTAL
.mg
.mg
.mg
_mg-
TOTAL WEIGHT
mg
MOISTURE
IMPINGERS -
FINAL VOLUME c ^ ml
INITIAL VOLUME ?*&>O ml
NET VOLUME ^6? ml
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
EPA (Dur) 231
4/72 " •
g
2£i
.g
.g
.g
g
g
g;
TOTAL MOISTURE
62
-------
NOMOGRAPH DATA
PLANT
DATE
SAIVIPLING LOCATION
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(P,n±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
T|"avg.
Bwo
rm
ps
Ps/pm
savg.
APavg.
APmax.
l.tf>
,7j
7°£>
7-9^
W.U$
1
/*$
AJ;
.^
• If
,->s
,^
T©5>
EPA (Dur) 234
4/72
63
-------
FIELD DATA
PLANT
DATE.
SAMPLING
SAMPLE TYPE H'
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE v
BAROMETRIC PRESSURE "~
STATIC PRESSURE, (P..) — .3 6
FILTER NUMBER (s) ^
' MOBE"LENGTH AND TYPE "3 G> I /
NOZZLE I.D
ASSUMED MOISTURE. '.
SAMPLE BOX NUMBER
METER BOX NUMBER _
METER AH
C FACTOR
, 7 X-
SCHEMATIC OF TRAVERSE POINT LAYJJUT
READ AND RECORD ALL DATA FVFRY .f> MINUTES
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE ip__
TRAVERSE
POINT
NUMBER
CLOCK TIME
GAS METER READING
VELOCITY
HEAD
(Aps), in. H20
ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H20)
DESIRED ACTUAL
STACK
TEMPERATURE
(TS).°F
DRY GAS METER
TEMPERATURE
INLET
(Tm in).°
OUTLET
PUMP
VACUUM.
in. Hg
SAMPLE BOX
TEMPERATURE.
°F
IMPINGER
TEMPERATURE.
"F
a / i / $30
.DQ
,0.
y/3/
/o
/Ofr
I.I?
/££
/ r
•3- 3 0 , 5 '5 0
y.
C
..I.I*-
(it
til
a.
p. 3 ^ . 5L '3 J5
in
£7
3.5
.75
7
• y- 3
.•>*•
rrr
9- V / ,
.19*
l/t?
-7f
no
C.
IO /(,.*$
" 10
It,
f /
J-L.
1.50
L5_C_
4-
±^.
1.50
toe
5.5
,3
IS?
/.tc
103
(s.C
0
*
,(? / 7. 01
. 75-5
Me
1.10
10 5
/o n.o-t,
I.3S
5'
57
^L
22.
I ,5
/,
IC7
J^L
IP /?.
7/
ft ~7
U)
55"
COMMENTS:
tPAiDut)235
-------
TRAVERSE
POINT
NUMBER
1
^\ CLOCK TIME
STTCUNG\^OC:hK>
TIME, mm X^
" — - — -__
5 17, t I
> 6 /7,f£
„
GAS METER READING
'V- «3
9-7 $ .IIC
-)~<6l .S^S
VELOCITY
HEAD
liip$). in. H^O
*«3
,+?
ORIFICE PRESSURE
DIFFERENTIAL
UK), in. HjO)
DESIRED
LSI
/.S-3
ACTUAL
/•5?
>>$!
STACK
TEMPERATURE
iTsl.°F
/ 05
/ a 5
DRY GAS METER
TEMPERATURE
INLET
.°F
e?
tc~
OUTLET
lT««».'-0|r
£V
e- &
PUMP
VACUUM.
in Hg
£,e
6 . &
SAMPLE BOX
TEMPERATURE.
°F
*>
rf-
IMPINGER
TEMPERATURE.
°F
-
EPA (Dur) 236
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT.
DATE.
COMMENTS:
SAMPLING TIME (24Vr CLOCK1 I JH 3 4
SAMPLING LOCATION ~D fr P '
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS)
ANALYTICAL METHOD /?/£ S
AMBIENT TEMPERATURE.
OPERATOR
ft/ /
O
^\^^ RUN
GAS ^^^
C02
O£(NET is ACTUAL o2
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING
a 4
HO
l/.o
fee, D
NET
'V
$0.0
?I.O
I-'". O
NET
0V
&J
0,0
77.0
i
ACTUAL
READING
'>?
?/,#
£/.#
tfo.O
NET
» +
?*>£
&^fr
7?,0
AVERAGE
NET
VOLUME
^
£#, £
o
~7
-------
ANALYTICAL DATA
PLANT
DATE_
MO.O
SAMPLING LOCATION ft A fr (GtAUO LftTMO)
SAMPLE TYPE F'
RUN NUMBER
SAMPLE BOX NUMBER _
flu
CLEAN-UP
AJ
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
LABORATORY RESULTS
CONTAINER.
CONTAINER
,mg
FRONT HALF SUBTOTAL
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
MOISTURE
IMPINGERS
FINAL VOLUME
-p / \
° ^ *
.ml
INITIAL VOLUME tZGO ml
NET VOLUME *> I ml
SILICA GEL
FINAL WEIGHT
g
INITIAL WEIGHT <£•&>. & g
NET WEIGHT /.<• g
EPA (Dur) 231
4/72
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
TOTAI WFIRHT
mg
mg
mg
itiE
-------
FIELD DATA
ON
00
PLANT f-\ r^<^<^
DATE '3/3_-5/-73
SAMPLING L
SAMPLE TYP
RUN NUMBEF
OPERATOR
nrimnN /3/J-P AS.ZTfH-K K
F /l//fo
1 t/^
PROBE LENGTH AND TYPE «* _^^ '
7 NOZZLE I.D.
^ ASSUMED MOISTURE. '. _
SAMPLE BOX NUMBER
AMBIENT TFMPERATURE <5~"2-
TRAVERSE
POINT
NUMBER
Trk
i
•3-i
? -
t/.
tj -
ft c
1 c>
o t
ID I
?
f"
~~
£
i
^
} (
y-T,
BAROMETRIC
STATIC PRE
FILTER NUM
\. CLOCK TIME
TIME.min ^v^
A^-^^
Cj ,6)^
5£
\0, 03>
' ^9
. 13
, (^
9.1
' 2.*f
» 33
' -^ U
If. 3
i ^4-\r
^PRFSSIIRF D.e// ^
KIIBF (P ) O, ~3 h
5 J /
RfR (c) ttf-
METER BOX
METER AHS
C FACTOR
!£tt U
^
NUMBER ^5
L
PROBE HEATER SETTING
HEATER BOX SETTING
V
REFERENCE *n — '—
1 SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA FVFRY 3 MINUTES
GAS METER READING
(Vm),lt3
£?,rt)E^
73, <3.i^
'7(c-i ^
.^n, s3i/
53, ^L
V7. ZJL/
• 9^« ^
• ILL. 5'U
9?- C-Q
/oV. 70'
/OS", ^7
/C5i ^^
•//si. ^9^
*
VELOCITY'
HEAD
(Aps), in. H20
^/ 1 1
^IfX? 1
'3v-o'/' */"-
'ifs*
'"S'Sl
~ ORIFICE F
DIFFER
(AH), ir
DESIRED
//,
/ f \
IS
l,*5
1 ' ^
1 ,
/iS>
/35"
f
> /7J
/
!'%
RESSURE
ENTIAL
.H20)
ACTUAL
t^
¥
4-
^7
I
LJ.
%LL
/j
t-%4-
''Su
£
$u
*L
STACK
TEMPERATURE
(T$).°F
{^T
/crD
'Ct
7^
C[~j
cld
Q.S
9^5
9/yC
cnl
95
°iU.
Q(/
•
DRY GAS METER
TEMPERATURE
INLET
"r^
^
U-
r ^
70
i/
73
~7'1
j5_l^_
7*4-
°7^
76
7£
OUTLET
"^V^
5'*r
55
Sic
5-1
^V"
to •
C;0
t /
^-'^.
C'( Q.
^ 3
c^u.
'
PUMP
VACUUM.
in. Hg
~&5~
^ SJ< 0
7.7s"
7-75
7' 75
-^ ^'0
-^'0
•vif-O
X^-O
•-#'0
-^•0
9'0
^9-0
SAMPLE BOX
TEMPERATURE.
fty
/^t-5
/^C;
A*?//?
I°i3.
l°l$
^?ro
/^"O
/C'<
//(]
/£#
/Q&'
zcto
IMPINGER
TEMPERATURE.
"F
-«*».,
~"^~iSi"- "
COMMENTS:
EPAiDut)235
-------
ANALYTICAL DATA
PLANT.
DATE:
SAMPLING i nrjmciN
SAMPLE TYPE
RUN NI1MRFR
SAMPLE BOX NUMBER
CLEAN-UP IVIAN
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
LABORATORY RESULTS
CONTAINER.
CONTAINER
.mg
.mg
FRONT HALF SUBTOTAL
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
MOISTURE
IMPINGERS
FINAL VOLUME
INITIAL VOLUME
NET VOLUME
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
EPA (Dur) 231
4/72
.ml
ml
.ml
CONTAINER
ETHER-CHLOROFORM
BACK HALF SUBTOTAL
.mg
.mg
.mg
_mg.
TOTAL WEIGHT
g
. g;
TOTAL MOISTURE
~L^
-------
NOMOGRAPH DATA
PLANT
DATE.
"if
SAMPLING LOCATION
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 * STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
Tmavg.
Bwo
Pn,
ps
Ps/Pm
savg.
APavg.
APmax.
IX&
73
7fe
z?,?
g*
/,0a
I/O
#'&?
^G,&
o.?
-------
FIELD DATA
PLANT.
DATE.
SAMPLING LOCATIONJ7 frr S
SAMPLE TYPE '' '
RUN NUMBER.
OPERATOR _
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE .
STATIC PRESSURE, (Ps)_-
FILTER NUMBER (s)
PROBE LENGTH AND TY
NOZZLE I.D
ASSUMED MOISTURE,',
SAMPLE BOX NUMBER
METER BOX NUMBER .
METER AHg, ,
CFACTOR
PROBE HEATER SETTING <£ £>
HEATER BOX SETTING
REFERENCE *r ,jT 1-
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY.
MINUTES
TRAVERSE
POINT
NUMBER
CLOCK TIME
GAS METER READING
(Vffl). It3
VELOCITY
HEAD
(Aps), in. H20
ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H20)
DESIRED ACTUAL
STACK
TEMPERATURE
(TS),"F
DRY GAS METER
TEMPERATURE
INLET
(Tmin),"F
OUTLET
7
76
/<30
y
if
2z.
t 1C
-4^
'[ (O
COMMENTS:
EPA (Our) 235
-------
*•/
TRAVERSE
POINT
NUMBER
4 /3
"N^ CLOCK TIME
ST3L1HG\CLOCK.
TIME. mm \^
~~ ___
5 /JL*3
/•O / z^K
GAS METER READING
'V- "3
34-/V b „
ii-j<-f,cilfr^
VELOCITY
HEAD
(ipjl. in. H20
O,?7>
£).?>'!-*
ORIFICE PRESSURE
DIFFERENTIAL
IAH). in. H20l
DESIRED
1*18
1,12-
ACTUAL
/,/&
///z-
STACK
TEMPERATURE
lTsl.°F
x/5"
//a
/
\
"* *
DRY GAS METER
TEMPERATURE
INLET
•In, JBI.«F
-7 ?
1 ^
OUTLET
lT»o»t'-°F
^,^
6,
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT
DATF
- It C O
COMMENTS:
SAMPLING TIME (24-hr CLOCK) / C> O 5 __
SAMPLING LOCATION J) fr ? M 6T??-£/< '?O/L /
J'/.
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD _
AMBIENT TEMPERATURE.
OPERATOR
^^^^^ RUN
GAS ^\
C02
Q£ (NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO (NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N 2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING
0,1^
y>3.
$o.<*
0
n*
2
ACTUAL
READING
0*1-
loj
?*.?
NET
O.Z^
->0,lo
O
It.Ts
3
ACTUAL
READING
&,?~- .
&•?
juh?
NET
d)-2-
^>.4
O
7*2-
AVERAGE
NET
VOLUME
6< 2^
30. Q
O
79,^
MULTIPLIER
44/100
!.._"."
32/100
_ ... i
^/lOO
a/ioo
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole
TOTAL
EPA (Dur) 230
4/72
-------
ANALYTICAL DATA
PLANT.
DATF 3 -
- 73
SAMPLING LOCATION Aft*
SAMPLE TYPE H\VAO J-i
RUN NIIMRFR
SAMPLE BOX NUMBER
CLEAN-UP MAN
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS), CONTAINER.
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER CONTAINER
LABORATORY RESULTS
.mg
.nig
FRONT HALF SUBTOTAL
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
MOISTURE
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
.mg
BACK HALF SUBTOTAL
mu.
TOTAL WEIGHT
««
IMPINGERS
FINAL VOLUME C
INITIAL VOLUME .
NET VOLUME _
SILICA GEL
FINAL WEIGHT t
INITIAL WEIGHT
NET WEIGHT
EPA (Dur) 231
4/72
- <-~ — ^ ml
S0O ml
3^5 m|
ff*8.
W-\ B
g e
E *
E *
74
TOTAL MOISTURE
-------
APPENDIX E
LABORATORY REPORT
This section presents the report on fluoride, ammonia, pH and
P205 analysis which were performed by EPA.
75
-------
SOURCE SAMPLE REQUEST & REPORT
(MUST BE FILLED OUT FOR EACH TEST RUN)
SAMPLING DATE Oa T 7 1
INDUS
COMF
ADDP
SAMP
IDENT NO
1
5)Z
. M rt\
I
|
1
1 ... -
YR MO DAY
TRY Tf^ifwM. /ju
(USE
ANY $.\t$ P-lLv~lt6t'
ESS ot-f. WlfiAuiA*-
1 ING fl5^ T@crusUj.ti
(00
FIRST IDENT.
NO. USED 5 ~?3 <&OO3"//
-Mj.ls^l/1,
TABLE A)
/
^i^a-
DESCRIPTION OF
SAMPLE OR SAMPLE
FRACTION
^ e^JeJta &»*+&
jtitA.M-'Htj^, ee>*ai*^> . [Lit*' y-^voui-/.
'3 1
COMMENTS:
SAMPLING
CONTRACTO
DATE OF REQU
TEST NO 73 FRTI
LAST IDENT.
NO. USED ^^3 OOoT/2. ' ^r.,
UNIT PROCESS OPERATIC
AIR POLLUTION CONTRC
FUEL USE
D INLET K 0
GAS VOLUME SAMPL
(METER VOL IN FT^
WT'
•(SOLID)
MG
SAM
JSJ//?
A//A
R -.-7/lJd«xd p.J&JlfuitJL ^(LA&fab PROJECT OFFICER
(IF APPLICABLE)
-ST y/?/7 ^ DATE ANA1 YSIS RF01IFSTED
PLE
VOL
(LIQUID)
ML
"2££>
fiir £^£"O
„-,„_•-)
/ • /r ff / >-*/-C-7^
N /^W*<^tf>t^i<»— 0Jt&L&fo<& RCRD. f 7 J -^
/ x ^
I Miidi&'O
COPIES TO
D /J/^yt-C p o~")
JTLET >• ^ -/? ' 73
^
TIT rn
ANALYSIS REQUESTED - GENERAL COMMENTS
(APPROX CONCENTRATIONS - POSSIBLE INTERFERENCES
ETC) (INDICATE SPECIFIC ANALYSIS ON BACKSIDE)
1
•SUMt **J JL*»&J6 1L<^U (12.2.^ *&jii/,e}
LtMi 6*sJ Jl*4*£j£ £Ww (C.C.^1 J^JL ^6 }
"
„
1 ' / /y //^ REQUEST YJ/ //
L^JUdt^^ -f^jJiVL REVIEWED RY y£-A -7V7^
V/tfh? DATE OF REQUEST
EPA(OUR)245
(TO BE FILLED IN BY SSFAB)
-------
RETWT OF ANALYSIS
TRACE ELEMENTS
ppm - for sol d samples
ug/ml - for liquid scmples
Mork (x) lor specific analysis
Mark (x) in block to leli of Went. No. when
requesting all analysis on the; line
rj-LtJ
Be
Cd ' As
UJ LU LJJ
Ni
CJ LJ LJ LJ LJ LJ LTTHJT
Cr
Zn
Cu
Pb
Se
irtj"
Li
Ag Sn
TTT
re
Sr
No
Co
Si
Mg
Ba
rjTTJ
F
L J
TT
UJ LJ LH
£
TT
EJ LU I II I l_Ll CJTITCJ UJ LLJ LTTIJ L_U l_Lj 1_J_I !_i-l LU LU
J~ I |^ [^ I !^ ! i^
LH
u
LJ
T±J
I I I I L J I I L J L J L
M-J
L_J L_LJ
'-H
^
•-H
I I LJJ I I I I I I LJ LJ LJ I I LJ LJ L
J LJ LjJ LJ
^F
I JL_T Lin I LJ I J L J LLTLJ LJH_JTI
^
JL
-S3
LJ UJ LJ_TLLT
U UJ UJ UJ
! i i
ET"Ltn:
I I LJ I I L J LJ1ZJ LJJ LJL
4^
L J L JL. JL. JL J L JL. JHZ
4^4^
4^
JL JL:J LJ i i i i uj i i LU u
u LLJ LLJTJJ LJJ LJ LJJ Limj i i L TT: nn j~n ITU TT: j~c un im TH im im im j LJJ IIITCJ i i LIT
i i^ i \^ i n^ i n^
rt
M
4
::ysis "eihoa': 1-NAA, 2-SSMS, 3-OES, 4-AA, 5-ASV, 6-XRF, and 7-other
Comments:
v jinclysis - Use Table S to fill analysis requested (oBove each column)
Marie (xi for specific o'aiysis requ?5;es
Idem No.
^ll
/.
JT
U
IT
IT
f-r
-------
••*, , ,mm>* i «• i »M*. i TRY P/LdL&. jLfi
^ (USE
AMY (JAZQ lAg/m^A
ESS M. 1fl\niQuerA.
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(TO BE FILLED IN BY SSFAB)
\r
-------
REPORT OF ANALYSIS
TRACE ELEMENTS
ppm • for so.id samples
ug/ml • for liquid samples
Work (x) for specific analysis
Mark (x) in block to left of ident. No. wnen
requesting all analysis on that line
idem Mo.
Hg
J L
J L
r-J L
J L
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Be
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1
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1
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r-J
1_
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Mn
J L
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Tr
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Ni
J L
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J L
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J L
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Sb
J L
J L
J L
J L
J L
J L
J L
J L
J
1
J L
Cr
J L
J L
J L
J L
J L
J L
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J L_
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Zn
J L
J L
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J L
J L
J L
J L
J L
J L
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Cu
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Pb
J L
J L
J L
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J L
J L
J L
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Se
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J L
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B
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F
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Ag
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Fe
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Sr
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No
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x
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SOURCE SAMPLE REQUEST & REPORT
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SAMPLING DATE
V3,
YR
3
MO
22
DAY
FIRST IDENT.
NO. USED
73 0005" 35"
LAST IDENT.
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17
INDUSTRY
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DESCRIPTION OF
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-------
REPORT OF ANALYSIS
TRACE ELEMENTS
ppm - (or soli:) somples
ug/ml - for liquid samples
Mork (x) for specific onolysis
Mork (x) in block to left of Ident. No. when
requesting oil onolysis on that line
~r.t f.'o.
Kg
HL
JU
J L
J L
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8?
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Mn
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Ni
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Til
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Sa
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J L
J L
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Cr
J L
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J L,
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J L
J L
J L
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Zn
J L
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J L
J L
J L
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J L
Cu
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Pb
J L
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J L
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J L
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Se
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B
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F ; Li
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Fe
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Sr
U L
J L
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J L
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No
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U L
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J 1_
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•:iysis Method: J-NAA. 2-SSMS, 3-OES, 4-AA, 5-ASV, 6-XRF, and 7-other Comments:
ner Analysis - U:e Table B to fill analysis requested (above eoch column)
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Mark (x) for specific analysis requested
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SOURCE SAMPLE REQUEST & REPORT
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REPORT OF ANALYSIS
TRACE ELEMENTS
ppm • (or solid somples
ug/ml • lor licuid samples
MCru (XI iUi iyui-nn, unuiyju
Mcrk (x) in block to left o! Ifient. No. v.-nen
recasting oil analysis on that line
i-;e-t No.
Hg
J L
J L^
M LJ
J L
J U
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Sb
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J L
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Cr
J L
J L
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J L.
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Zn
J L
J L
J L
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J L
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Cu
J L
J L
J L
J L
J L_
J L.
J L
J L
J L
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Pb
J L
J L
h1 L
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h1 L
J 1_
J L
J L
J L
Se
J L
J L
nJ L
J L
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Analysis Method: 1-NAA, 2-SSMS. 2-OF.S, 4-AA, 5-ASV, 6-XRF, and 7-other Comments:
Other Anc-iysis - Use Toble B to fill analysis requested (above each column) Mark (x) for
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Comments:
-------
DATE 73! ^ |?3
YR MO DAY
INDUSTRY P/iupJiAA,
COMPANY Afco (It*
AMRFSS „£/. #//V^L
SAMPI ING £-Prl &&H.
METHOD
SOURCE SAMPLE REQUEST & REPORT
(MUST BE FILLED OUT FOR EACH TEST RUN)
TFQT NO ??-rer-/
FIRST IDENT.
NO. USED 3-73 000 «-9
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NO. USED 0 7E ooo SC.2 RilHHn ^
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ANALYSIS REQUESTED - GENERAL COMMENTS
(APPROX CONCENTRATIONS - POSSIBLE INTERFERENCES
ETC) (INDICATE SPECIFIC ANALYSIS ON BACKSIDE)
&JM. +***dJ£ ' SA»fiieh / 12* *J *&,_jL jfei
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SAMPLING
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-j (IF APPLICABLE)
"-! DATE OF RFQIIFST »/»/? J
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.DATE ANALYSIS REQUESTED..
DATE OF REQUEST.
(TO BE FILLED IH BY SSFAB)
-------
RTTCHT OirAM.YSIS
TRACE ELEMENTS
ppm - for solid samples
ug/ml - for liquid samples
Mork (x) for speciiic G;,a!ysjs
Mor1< (x) jn b|OC|< to |eft o! !t!ent. NO- wf,en
requesting all analysis on that line
:ent No.
Hg
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Be
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Cd
J L
J L
J L
J L
J L
LJ L
J L
J L
J L
As
J L
J L
J L
J L
J L
J L
J L
J L
J l_1
J LJ L
V
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Mn
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Ni
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Sb
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Cr
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Zn
J L
J L
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Cu
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Pb
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Hg
r1 ^
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J L
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J L
V
J L
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J UJ L
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
J UJ 1 1 U
Mn
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Ni
J L
J L
J L
J L
J L
J L
J L
J L
J L
J" L
Sb
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Cr
r-1 L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Zn
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Cu
J L
J L
J L
J L
J L
J L
rJ L
J L
J L
J L
Pb
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Se
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
B
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
F
J L.
J L.
J L
J L.
J L
J L.
J L.
J L.
r-l L
J L
Li
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J L
J L
J L
J L
J L
J L
J L
J L
J L
Ag
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Sn
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Fe
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
Sr
J L
J L
J L
J L
J L
J L
J L
J L
J L
J L
No
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J L
J L
J L
J L
J L
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Mg
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J L
J L
J L
J L
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J L
J L
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J L
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REPORT OF ANALYSIS
TRACE ELEMENTS
ppm - (or solid samples
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TRACE ELEMENTS
ppm • for solid somples
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Mark (xl 'or^specific onslysis •
Work (x) in bloc* to ieit o! Icent. No.
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Cr
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J L
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Zn
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Cu
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Pb
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SOURCE SAMPLE REQUEST & REPORT
(MUST BE FILLED OUT FOR EACH TEST RUN)
SAMPLING DATE
73
YR
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LAST IDENT. 375 ooo
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WT VOL
(SOLID)
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ANALYSIS REQUESTED - GENERAL COMMENTS
(APPROX CONCENTRATIONS - POSSIBLE INTERFERENCES
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DATE OF REQUEST.
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REQUEST
-REVIEWED BY
DATE ANALYSIS REQUESTED
DATE OF REQUEST.
(TO BE FILLED IN BY SSFA8)
-------
REPORT OF ANALYSIS
TRACE ELEMENTS
ppm - for solid somples
ug/ml - for liquid somples
Work (x) for specific onolysis
Work (x) in block to left of Ident. No. wrier,
requesting oil analysis on triot line
~~\. Nc
Hg
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SOURCE SAMPLE REQUEST & REPORT
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SAMPLING DATE 0^ 1 '*.'*-
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KF.POKI OP ANALYSIS
TRACE ELEMENTS
ppm - lor solid somples
ug/ml • for liquid samples
Mark (xt lor specific dialysis
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SOURCE SAMPLE REQUESTS REPORT •
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SAMPLING DATE
INDUSTRY
COMPANY
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D INLET D OUTLET
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LAG.
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IDENT NO
ANALYSIS REQUESTED • GENERAL COMMENTS
(APPROX CONCENTRATIONS - POSSIBLE INTERFERENCES
ETC) (INDICATE SPECIFIC ANALYSIS ON BACKSIDE)
DATE ANALYSIS RFQIIFSTFn
DATE OF REQUEST
H EPA(OUR)245
Jl _..,_:
(TO BE FILLED IN BY SSFA3)
-------
UT
TRACE ELEMENTS
ppm • (or solid somples
ug/ml • for liquid samples
Mo:X U> lor specilic onci/sis
Merit (x> in block to left of Idem. No. when
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.'i.AA. 2-SSMS, 3-OES. 4-AA, 5-A5V, 6-XRF. and 7-other
itter Analysis - Use Table B to fill analysis requested (oBcve each column)
Mark (x) for specific onclysis
-------
APPENDIX F
TEST LOG
Table F-I presents the actual time during which each sampling was
done.
104
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TABLE F-l
SAMPLING LOG
Run
F-1A
F-l
1
NH3-1
F-1,NH3-1
F-2
F-2
F-2
F-2
F-2
NH3-2
F-2,NH3-2
F-3
F-3
F-3
F-3
F-3
NH3-3
F-3,NH3-3
F-4
F-4
F-4
F-4
F-4
F-4
F-5
F-5
F-5
F-5
F-5
NH3-4
F-5,NHo-4
Location
Stack
Stack
n
n
ii
n
n
Various
Stack
n
n
n
n
n
Various
Stack
n
n
n
n
n
Various
Stack
n
n
n
"
Various
Stack
n
n
n
n
n
Various
Port
1
1
2
3
3
4
4
-
1
2
3
3
4
4
-
1
2
1
3
4
4
-
1
2
3
4
4
-
1
2
3
3
4
4
-
Pollutant
Temperature
and velocity
Fluoride
Fluoride
CO,C02j02
Fluoride
Fluoride
Ammonia
Liquid/Solid
Fluoride
Fluoride
co,co2,o2
Fluoride
Fluoride
Ammonia
Liquid/Solid
Fluoride
Fluoride
co,co2,o2
Fluoride
Fluoride
Ammonia
Liquid/Solid
Fluoride
Fluoride
Fluoride
co,o2,co2
Fluoride
Solid/liquid
Fluoride
Fluoride
CO,C02,02
Fluoride
Fluoride
Ammonia
Liquid/Solid
Date
3-20-73
3-21-73
n
"
n
"
11
"
it
n
n
n
n
"
n
3-22-73
n
n
n
n
n
n
n
n
n
ii
n
n
3-23-73
n
n
"
n
it
n
Time
Began-Ended
15:00-15:20
10:52-11:25
11:44-12:35
11:50-12:20
12:45-13:15
13:25-13:55
10:58-11:58
11:00-13:45
16:04-16:34
16:45-17:15
16:20-16:50
17:23-17:53
18:00-18:30
16:10-17:10
16:10-18:10
10:04-10:34
10:44-11:14
11:08-11:38
11:24-11:54
12:13-12:43
11:01-12:01
10:10-12:10
15:20-15:50
15:58-16:28
16:38-17:08
15:34-16:04
17:16-17:46
15:30-17:30
09:39-10:09
10:19-10:49
10:05-10:35
10:58-11:28
11:38-12:08
09:48-10:48
09:45-12:00
Elapsed
Time
(min)
20
33
51
30
30
30
60
165
30
30
30
30
30
60
120
30
30
30
30
30
60
120
30
30
30
30
30
120
30
30
30
30
30
60
135
105
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APPENDIX G
PROJECT PARTICIPANTS AND TITLES
106
-------
Name
Paul Constant
Pat Shea
Reid Flippin
Henry Moloney
Bill Maxwell
Mike Bechtold
Bill Cunningham
Christine Guenther
Title
Program Manager
Project Chief
Testing Engineer
Laboratory Technician
Process Sampler
Engineering Technician
Testing Engineer and
Engineering Technician
Laboratory Technician
Engineering Technician
Programmer
107
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