TEST NUMBER 73-CRN-1
RALSTON PURINA COMPANY
LOUISVILLE, KENTUCKY
PEDCo ENVIRONMENTAL
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TEST NUMBER 73-CRN-1
RALSTON PURINA COMPANY
LOUISVILLE, KENTUCKY
Prepared by
Richard W. Gerstle, P.E.
and
Robert S. Amick
EPA Project Officer
Thomas E. Ward
PEDCo-Environmental Specialists, Inc
Cincinnati, Ohio
Contract No. 68-02-0237, Task 17
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I. TABLE OF CONTENTS
Page Number
II. INTRODUCTION 1
III. SUMMARY OF RESULTS 4
IV. PROCESS DESCRIPTION 12
V. PROCESS OPERATION 16
VI. LOCATION OF SAMPLING POINTS 17
VII. SAMPLING PROCEDURES 21
APPENDICES
A. PARTICULATE RESULTS AND CALCULATIONS
B. GASEOUS RESULTS
D. FIELD DATA . •' • .
E. SAMPLING PROCEDURES
F. LABORATORY REPORT
G. TEST LOG
I. PROJECT PARTICIPANTS AND TITLES
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II. INTRODUCTION .
Tests Performed
A series of tests were conducted at the Ralston Purina
Company, Chow Division Plant in Louisville, Kentucky on
November 6 and 7, 1972. Tests were made to determine particu-
late concentrations at the inlet and outlet to the pellet
cooler cyclone and at the outlet of the hammermill cyclone.
Stack gas velocities, temperature, and moisture content were
also measured during each test. Table 1 summarizes the test
locations, dates and the measurements made.
Sampling Sites
Figure 1 shows the sampling site locations. Stack gases
were sampled for particulate concentration before and after
the cyclone serving the pellet cooling operation at Points A
and B iri Figure 1. The outlet site was located in a temporary
duct which had been added to the cyclone to provide a suitable
sampling site. Normally the cyclone is vented directly to the
atmosphere from the fan. . •
The outlet to the hammermill cyclone was :also sampled for
particulate matter. Sampling was done at point C as shown in
Figure 1, by using a temporary cyclone outlet stack extension.
The cyclone, as normally operated, had.a rain cap (Chinaman's
hat) placed over the outlet.
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TABLE 1
SUMMARY OF EMISSION MEASUREMENTS MADE AT
RALSTON PURINA COMPANY IN LOUISVILLE, KENTUCKY
DATE
1972
11/6
11/6
11/6
11/6
11/6
11/6
11/7
11/7
11/7
TEST
NO.
1
2
3
4
5
6
7
8
9
TEST
SITE
Pellet Cooler Cyclone Inlet
Pellet Cooler Cyclone Outlet
Pellet Cooler Cyclone Inlet
Pellet Cooler Cyclone Outlet
Pellet Cooler Cyclone Inlet
Pellet Cooler Cyclone Outlet
Hammermill Cyclone Outlet
Hammermill Cyclone Outlet
Hammer mi 11 Cyclone Outlet
STACK GAS PARAMETERS EMISSIONS
Velc
city Te
' i
jmp. %H
1 - i
20 Parti
1
^ulate
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\
i
i
• B
I
Pellet Cooler
Hanunermill
Figure 1. Sampling Sites - Ralston Purina Co., Louisville, Kentucky
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III. SUMMARY OF RESULTS . .
Tables 2 through 6 summarize the stack gas parameters,
and the emission,process, and sampling data obtained during
this test series. Additional data, calculations, and original
field data are included in the Appendices to this report.
Pellet Cooler
Table 2 contains the stack gas and particulate emission
data for the pellet cooler at the inlet and outlet of the
cyclone serving this operation. The slightly higher gas flows
at the outlet site, as compared to the inlet site, are probably
due to the leakage of outside air into the duct work around
the fan shaft and housing.
Two values are reported for the particulate concentrations
and emissions. The value designated as "front" represents the
particulate collected in the front half of the sampling train,
namely, the probe and filter. The "total" value is the entire
amount of particulate collected in the train, namely the front
half and the material collected in the impingers. The amount
collected in the impingers (organic extract and inorganic
residue) amounted to an average of 2% of the total particulate
collected at the inlet site and 32% at the outlet. .
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TABLE 2. PELLET COOLER EMISSION DATA SUMMARY
RALSTON PURINA COMPANY, LOUISVILLE, KENTUCKY
November 6, 1972
Test'
No. Time Site
1 13:30 Inlet
to
2 15:45 Outlet
3 16:20 Inlet
to
4 18:30 Outlet
5 19:20 Inlet
to
6 21:40 Outlet
Stack Gas Parameters
Velocity
FPS
57.1
44.5
55.9
44.7
53.3
44.3
Temp.
°F.
94
90
92
90
90
86
Moisture
%
2.2
2.5
2.0
1.9
2.2
2.3
Volume
SCFM
15,495
16,085
15,200
16,167
14,538
16,057
Particulate Emissions
Concentration
Grs./SCF
Front Total
.3616 .3696
.0159 .0250
.4074 .4161
.0143 .0213
.5020 .5083
.0128' .0175
Pounds/Hour
Front Total
48.019 4.9.075
2.149 3.445
53.066 54.197
1.976 2.948
62.546 63.335
1.765 2.409
Pounds /Ton
Front Total
4.99 5.10
.223 .358
5.51 5.63
.205 .306
5.80 5.87
.164 .223
(a) Inlet and outlet to cyclone collector
(b) Standard cubic feet per minute, dry basis corrected to 70°F. and 29.92 Hg.
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TABLE 3. PELLET COOLER PRODUCTION DATA
Run
No.
Test
No.
Feed
Composition, %
Feed
Rate, Pounds/Hour
1
2
1,2
3,4
5,6
40% Ground Corn
30% Wheat Middlings
5% Minerals
20% Grain By-Products
5% Molasses
65% Ground Corn
25%-30% Soybean Meal
5% Minerals
2% Animal By-Products
19256
20575'
22550
(a) Rate during first hour of a two-hour test.
(b) Rate during second hour; average rate = 21563
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TABLE 4. SUMMARY OF LABORATORY RESULTS AND SAMPLING DATA
RALSTON PURINA COMPANY - PELLET COOLER
Test Number
1
2
3
4
5
6
Meter Volume
SCFDa
83.246
60.883b
78.364
107.546
78.706
110.894
P articulate
Front
Found, mg
Total
1950.9
61.5
2068.9
99.4
2560.7
92.2
1993.8
98.6
2113.0
148.3
2593.0
125.8
%
Isokinetic
107
102
107
101
108
104
a) Standard Cubic Feet, Dry Basis Corrected to 709 F and 29.92" Hg.
b) Smaller Sized Sampling Nozzle Used During This Run
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TABLE 5. HAMMERMILL EMISSION DATA SUMMARY
RALSTON PURINA COMPANY, LOUISVILLE, KENTUCKY
November 7, 1972
Test
No. Time
7 12:30 to 15:30
8 16:20 to 17:00
9 18:30 to 19:40
Stack Gas Parameters a
Velocity
FPS
52.5
57.0
62.1
Temp.
°F.
72
78
76
Moisture
%
1.7
1.5.
1.7
K;
Volume
SC.FM .
5,316
5,713
6,240
. Particulate Emissions
Concentration
Grs./SCF
Front Total
.025.3. ..0335
.0192 .0252
.0153 .0212
Pounds /Hour
Front Total
1.151 1.525
.938 1.234
.817 1.133
Pounds/Ton
Front Total
.144 .191
.117 .154
.102 .142
CO
(a) Cyclone Outlet
(b) Standard cubic feet per minute, dry basis corrected to 70°F. and 29.92" Hg.
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TABLE 6. SUMMARY OF LABORATORY RESULTS AND SAMPLING DATA
RALSTON PURINA COMPANY - HAMMERMILL CYCLQNE OUTLET
Test Number
7
8
9
Meter Volume
SCFDa
80.471
46.469
50.419
Particulate
Front
131.8
57.7
49.9
Found , mg
Total
174..6
75.9
69.2
%
Isokinetic
111
115
114
a) Standard cubic feet per minute, dry basis corrected to 70°F and 29.92 "Hg.
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Table 3 summarizes the pellet composition and production
rate for each of the test runs. The first two runs (Test 1,
2, 3 and 4) were essentially identical from a production view-
point. A dairy feed was produced during the first two runs at
an average rate of 9.628 tons per hour. During the third run,
two types of turkey feed were produced. The two feeds differed
only in the amount of soybean meal, with the feed produced during
the second hour of this run containing about 5% more Soybean meal,
During the switch from one feed to another, sampling was dis-
continued. The average process rate was 10.7815 tons per hour.
The data in Table 2 show that particulate emissions from
the process increased during the three runs. Process weight
rates were identical for the first two runs but increased during
run 3. The total particulate emitted from the cyclone averaged
0.0212 grains per SCF, 2.934 pounds per hour, and 0.296 pounds
per ton of product. Average cyclone efficiency, based on pounds
of total particulate was 94.6%. There were no visible emissions
from the cyclone outlet. Variations in efficiency are probably
due to particle size variations.
Table 4 presents the laboratory results for each run, the
volume of gas sampled and the percent of isokinetic sampling
rate for each of the six tests on the pellet cooler. Each test .
extended over approximately a two hour period.
10
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Hammermill
Table 5 presents a summary of stack gas parameters and
particulate emission data for the hammermill cyclone outlet
sampling site. An average of 1.3 pounds of particulate
(0.162 pounds per ton of product) were emitted from this
cyclone at a concentration of 0.0266 grains per standard
cubic foot. A production rate of 8 tons per hour was maintained
during all tests. The opacity was 5% white.
An average of 75% of the particulate matter was found
in the front half of the sampling train. Table 6 presents
a summary of the sample volumes, laboratory results, and
percent of isokinetic sampling rate. Sampling times were
two hours for test 7 and 64 minutes each for tests 8 and 9.
This sampling site contained two points which had negative
velocity head readings due to the cyclonic nature of the flow.
This flow pattern limits the accuracy of the total .stack gas
flow as measured with a pitot tube.
11
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IV. PROCESS DESCRIPTION
Pellet Cooling
A wide variety of cattle and poultry feeds are manufactured
in both checker and pellet form at this plant. In the pelletizirig
process tested, ingredients are mixed in a batch, and gravity
fed to a California Pellet Mill where they are formed into
small cylindrical pellets. As shown in Figure 2, the pellets
then drop into a double-pass, horizontal cooler through which
room air is drawn to cool and partially dry the warm pellets.
(California Pellet Mill Co., Model No. 5 HR 34DD, Serial No.
232828). This cooler consists of two continuous perforated
belts with an effective width of 34 inches and length of 60 inches.
Dust entrained in the cooling air is collected in a Longhorn
No. 79 cyclone collector and the cleaned air vented directly
to the atmosphere. A 30 horsepower fan operating at 1330 rpm*
was mounted at the cyclone outlet.
Fines collected in the cyclone are recycled to the
pellet mill.
Hammermill
Whole kernel corn is pulverized by hammermills for use as
a basic feed ingredient. A number of hammermills are used at
this plant. The unit tested was a Prater, size 9, style COS
(Serial No. 22469) , as shown in Figure 3.. Cracked kernels
* not measured.
12
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Longhorn #79
Cyclone
Sampling
Site A
Duct extension
and transition
from rectangular
to round
I (
L Sampling Site B
I
Pellet Cooler
Figure 2. Pellet Cooler
13
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Kice Dual
Cyclone Collectors
18 "0 Cyclone Duct
Extension
To storage
Corn
Prater Hammermill
N
y
I I
• o, i Sampling Site C
Figure 3. Hammermill System
14
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are then pneumatically conveyed by a 50 horsepower blower
to two cyclone collectors mounted in series. The cyclone
collection system is a Kice, Model 2 SPW 16-8. The product
is collected in the cyclones, and fines are vented to the
atmosphere.
15
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V. PROCESS OPERATION
Pellet Cooler
The pellet cooler operated in a normal manner.
Feeds were chosen which provided long runs, i.e. about
2.5 hours. The composition of the feeds was previously shown
in Table 3. The pellet mill operated at a power input of
130-150 amps during the first run and for 75% of the second
run and then dropped off slowly to 110 amps.
The addition of a cyclone extension did not apparently
effect the cooling air rate through the unit.
Hammermill
The hammermill operated continually in a normal manner.
During each of these tests, Number 2 yellow corn with 2% FM was
ground at a steady rate of 8 tons per hour. The hammermill
operated at 1800 rpm, and a size 12 screen was used to yield
a course grind. A sieve analysis of the ground corn yielded
the following data:
Tyler Screen Size % Retained
8 5.5 '
24 58.5-65.0
42 85.5-87.5
The addition of the cyclone extension did not apparently
affect the air flow through the process.
16
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VI. LOCATION OF SAMPLING POINTS
Figures 4 , 5, and 6 show the sampling ports and the
number of sampling points at the sites used to determine
emissions from these two operations. As shown in Figure 4, .
the pellet cooler cyclone inlet samples were collected at
32 points (16 along each diameter) in the 30 inch round
vertical duct. This port was 5.1 diameters upstream from
the bend leading into the cyclone and 5.2 diameters down-
stream from the transition duct leading from the pellet
cooler hood. Figure 5 shows the pellet cooler cyclone out-
let sampling site and the 36 traverse points (18 along each
diameter) in the 34.5 inch round vertical duct. This port
was located in the temporary duct extension and was 3.33
diameters downstream from the transition section and bend
(duct changed from rectangular to round), and 0.83
diameters upstream from the duct outlet.
Figure 6 shows the hammermill cyclone outlet site and
the 16 points (8 along each diameter) in an 18 inch round
vertical duct. The sampling ports were 2 diameters upstream
from the duct exit and 4.7 diameters downstream from a bend.
17
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To cyclone Inlet
A
Roof
/ / /
o
30"
7V
_V
From
Pellet
Cooler
///Y/7
156 "
153"
Point
1
2
3
4
5
6
1
8
9
10
11
12
13
14
•15
16
Distance to
Traverse Point,In,
1.0
1.5
2.6
3.8
5.1
6.6
8.5
11.3
18.8
21.5
23.4
24.9
26.3
27.5
28.5
29.0
N
Section AA
N
FIGURE 4. PELLET COOLER CYCLONE INLET SAMPLING LOCATION
18
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Point
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
Distance to
Traverse Point, In,
1.0
1.5
2.6
3.8
5.0
6.5
8.1
10.2
13.2
21.3
24.5
26.4
28.0
29.5
30.7
31.9
33.0
33.3
Cyclone Outlet
V
\l
\
115"
SW
Section AA
t
A
O
34.5"
A .
29"
FIGURE 5. PELLET COOLER CYCLONE OUTLET SAMPLING LOCATION
19
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Cyclone Outlet
Distance to
Point Traverse Point, In,
1 1.0
2 1.9
3 3.5
4 5.8 .
5 12.2
6 14.5
7 16.1
8 17.0
87"
W
N
Section AA
North
o
18"
1
A
36"
A
FIGURE 6. HAMMERMILL CYCLONE OUTLET SAMPLING LOCATION
20
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VII. SAMPLING PROCEDURES
All sampling procedures were selected by EPA prior to
field sampling. The analysis of collected samples was per-
formed by PEDCo. Original data sheets arid associated velocity
and sampling volume calculations are included in Appendix D.
/
Velocity and Gas Temperature
All gas velocities were measured with a type S pitot
tube and inclined draft gage. In all cases velocities were
measured at each sampling point across the stack diameter to
determine an average value according to procedures described
in the Federal Register - Method 1. Temperatures were
measured by long stem dial thermometers.
Particulates
Method 5 as described in the Federal Register 1 Was
used to measure particulate matter. A glass, lined probe,
fiber glass filter, and impingers containing distilled water
were used as shown in Figure 7. The fourth impinger contained
silica gel. The sampling cyclone was hot used except for
Test 1. Due to low moisture content and near ambient stack gas
temperature, probes and filters were not heated during the
tests.
1) Federal Register, Vol. 36, No. 247, Part II Dec. 23, 1971
21
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Filter
Thermometer
to
to
Glass
Probe
100 ml of water1* Silica
Calibrated Orifice
Ice Bath
Figure 7 . Particulate sampling train.
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In all cases sampling was conducted under isokinetic
conditions by continually monitoring the velocity with a
pitot tube and adjusting the sampling rate accordingly with
a three-independent-variable nomograph.
The train cleanup procedure consisted .of measuring the
water collected and weighing the silica gel to determine
moisture content. The water was then poured into a glass
jar. The filter was removed and placed in marked container.
The probe and front half of the filter holder were then rinsed
with analytical reagent grade acetone and the washings placed in
a glass container. The rear half of the train consisting of
filter holder, impingers, and connectors were rinsed with
distilled water and this water added to the impinger contents.
The rear half of the train was then rinsed with acetone and
placed in a third sample jar. A portion of the acetone and
distilled water used in the sample recovery, were set aside and
used as blanks for analysis. . .
Analysis followed the procedures described in Method 5
of the Federal Register of August 17, 1971. This consisted
of:
1. Drying the filter in a desiccator at room temperature
and weighing.
2. Federal Register, Vol. 36 No. 159 Part II, AUg. 17, 1971.
23
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2. Transferring the acetone washings from the probe
and front half of the filter holder to a tared
beaker and evaporating to dryness at room temperature
and weighing.
3* Extracting organics from the impinger water and wash-
ings with chloroform and ether. The extracts were
placed in a tared beaker and dried at room temperature
and then weighed.
4. The remaining water was placed in a tared beaker
and evaporated by boiling. The residue was weighed.
5. Transferring the acetone washings from the rear half
of the train to a tared beaker, evaporating to dryness
at room temperature and weighing.
24
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Appendix A
Particulate Results
and Calculations
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TEST DATA SUMMARY SHEET
Ralston Purina
City Louisville, Kentucky Test Site Pellet Cooler
Test No.
Date 1972
Time
Meter Volume, C.F.
AH Avg. "H00 Avg.
Meter Inlet Temp. °F
Meter Outlet Temp. °F
Pump Vacuum "Hg
Filter Temp. °F
Impinger Temp. °F
Test Time, Min .
Barometric Press. "Hg
Stack Gage Press. "H00
Stack Gas Temp. °F
Stack Area, Ft.
Nozzle Size, Inches
Molecular Weight
% Moisture
Sample Volume SCFD
Stack Gas Velocity FPS
Stack Gas Volume SCFM
Stack Gas Volume SCFMD
% Isokinetic
Particulate Found, mg
Probe
Filter
Impinger Organics
Impinger Residue
Total
1
ii-6
1320-1536
88.374
1.34
104
92
4.9
N/A
65
128
29.58
-1.20
94
4.909
0.1875
28.76
2.24
.8 3. .2 4 .6
57.1
15.,849
JL5/.495
107.4
1950. 83
0.1
36.2
6.7
1993. 8
2
1 1-fi
1340-154!
66.257
0.62
119
103
4.7
N/A
66
126
' 29.58
-0.42
90
6.492
0.1875
28.73
2.53
60. .883
44.5
16,502
16,085
101 . 7.
61.3
0.2
28.3
8.8
98.6
3
ii-6
1 1625-183C
82.529
1.25
.98
85
7.1
N/A
58
123.6
29.45
-1.20
92
4.909
0.1875
28,78
2.05
78.364
55.9
15,518
15,200
106.8
809.5
1259.4
37.8
6.3
2113.0
4
11-6
1620-183;
118.612
1.93
130
107
4.7
N/A
71
126.0
29.45
-0.42
90
6.492
n ?snn
28.79
1.97.
107. 54?
44.7
16,494
16,169
100.5
93.0
6.4
41.6
7.3
14 S. 3
1. Sum of ether and chloroform extract, and acetone rinse
2. Residue from evaporation of extracted impiriger water
3. Includes cyclone
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TEST DATA SUMMARY SHEET
RALSTON PURINA
City
. Louisville ,
Kentucky
T^.Qt- No.
5
Test
Site
6
Pellet
Cooler
Test No.
Date 1972.
Time
Meter Volume, C.F.
AH Avg. "H00 Avg.
Meter Inlet Temp. °F
Meter Outlet Temp. °F.
Pump Vacuum "Hg
Filter Temp. °F
Impinger Temp. °F
Test Time, Min.
Barometric Press. "Hg
Stack Gage Press. "H00
Stack Gas Temp. °F
Stack Area, Ft.
Nozzle Size, Inches
Molecular Weight
% Moisture
Sample Volume SCFD
Stack Gas Velocity FPS
Stack Gas Volume SCFM
Stack Gas Volume SCFMD
% Isokinetic
Particulate Found, mg
Probe
Filter
Impinger Organics
Impinger Residue
Total
i
11-6
1920-2141
81.735
1 . 13
92
79
4.0
N/A
62
128
29.55
-1.55
90
4.909
0.187!
28.75
2.27
78.700
53.3
.14/876
14/538
108.1
2558.4
2.3
26.. 4
5.9
2593.0
b
11-6
> 1920-2135'
121.244
1.91
124
101
4.6
N/A
77
126
29.40
, -.42
86
6.492
i 0.2500
' 28.75
2.30
110.894
44.3
16-7436
16V 059
104-.3-
91.3
0.9
29.0
4.6
125.8
1. Sum of ether and chloroform extract.and acetone rinse
2. Residue from evaporation of extracted impinger water.
-------
TEST DATA SUMMARY SHEET
Ralston Purina
City Louisville, Ky. Test Site Hammermill
Test No.
Date
Time
Meter Volume, C.F.
AH Avg. "H^O Avg.
Meter Inlet Temp. °F
Meter Outlet Temp. °F
Pump Vacuum "Hg
Filter Temp. °F
Impinger Temp. °F
Test Time, Min .
Barometric Press. "Hg
Stack Gage Press. "H.,0
Stack Gas Temp. °F
Stack Area, Ft.
Nozzle Size, Inches
Molecular Weight
% Moisture
Sample Volume SCFD
Stack Gas Velocity FPS
Stack Gas Volume SCFM
Stack Gas Volume SCFMD
% Isokinetic
Particulate Found, mg
Probe
Filter
Impinger Organics
Impinger Residue
Total
7
11-7
1230-153C
84.049
1.28
91
73
2.7
N/A
65
120.0
29.20
-.31
72
1 .7fi7
0.1875
28.81
1.71
80.471
52.5
5409
5316
11.1 . 3
129.2
2.6
37.3
5.5
174.6
8
11-7
1620-180C
49.786
1.39
106
86
4.6
N/A x
62
64
29.20
-.27
78
1.767
0.1875
b 28.84
1.52
46,469
57.0
5*00
5712
114.7
54.8
2.9
13.0
5.2
75.9
9
11-7
1830-1940
51.758
1.59
82
64
4.0
N/A '
62
6.4
29.20
-.27
76
1.767
0.1875
28.81
1.76
50.419
62.1
6352
6240
114.1 -
49.3
0.6
6.6
12.7
69.2
1. Sum of ether and chloroform extract, and acetone rinse,
2. Residue from evaporation of extracted impinger water.
-------
of
2, Volu»"v\e. orr uJI'tOr • - - — - ° ~>™ «»•»
-. 0,
3, %
100
\/
u,
160 *
-------
4-.
100- %> W\
VOO
100
5",
NOT
-------
r/. vt^cAv. vje-\ ocvVvj $ tta.cXv.; d-oo
-------
rvt
V-
II.
( .-
x
* O.OISA-2Z.
. s
KIOT
-------
^ 4
6,00851
IS",
-------
APPENDIX B.
GASEOUS RESULTS
No gaseous emissions were measured during this test series.
Air was the only gas flowing in this process system.
-------
APPENDIX D. FIELD DATA
The field data sheets included in this appendix consist
of the original data sheets and computer print-outs of these
data along with associated calculations for moisture, meter
volume, and stack gas flow.
-------
FIELD DATA
PLANT
SAMF
SAMF
OPES
AMB1
BAR.
RALSTON
'LING LOCATION PELLET
>LE TYPE " " ~ "" PARTICU
iATOR R S AMI
ENT TEMP.tDEG.F) 60
PRESS. ( IN. HG) 29.56
PURINA, LOUISVILLE. KY.
COOLER-INLET
LATE
CK
DATE
RUN NUMBER
11/06/72
1
PROBE LENGTH AND TYPE 36 INCH GLASS
NOZZLE I.D. .1875
ASSUMED MOISTURE 2
SAMPLE BOX NUMBER 0
STATIC PRESSUN.H20) -1.20
FILTER NUMBERISI 200053
STACK INSIDE DIM(IN) 30.000
PITOT TUBE COEFF .85
READ AND RECORD DATA EVERY 4
TRAVERSE
POINT
NO.
INIT
N-l
2
3
4
5
6
.. . . ^
e
9
10
11
12
' 13
14
- -15
16
E-i
2
... 3
4
. s
6
7
e
" 9 ""
10
11
•12.;-
': -13 ••"
;14
15
16
"TOTALS "•"""
AVERAGE •
SAMPLE
"TIME
(MIN.)
0
" 4. "
8.0
12.0
16.0
20.0
24.0
28.0
32.0
" 36.0
40.0
44.0
48.0
52.0
96.0
60.0 "
64.0
68.0
72.0
76.0
80.0
84.0
88.0
92.0
96.0
ioo.o
104.0
108.0
1)2.0
116.0
120.0
124.0
128.0
128.0
CLOCK GAS METER
TIME " READING
(24-HR (CU.FT.)
CLOCK)
1320 156.680
159.123
161.448
163.916
166.521
168.996
171.663
174.441
177.164
180.044
183.114
186.019
188.995
191.954
194.962
" " 197.955
200.896
1432 203.000
205.226
207.483
209.854
'212.314
214.754
217.424
220*064
223.000
226*041
229.121
232*231
: 235*496
238.666
241.841
1536 245.054
88.374
MINUTES
VELOCITY
HEAD
UN.H20)
.650
.700
.800
.800
.840
.940
.940
.970
1.100
1.150
1.100
1.100
1.100
1.100
1.100
1.100
.540
.570
.650
• 670
'•" ".750
.790
.870
.94.0
1.1 oo
1.150
1.160
1.200
1.200
1.200
1.200
1.150
ORIFICE
DIFFE
I IN.
DESIRED
" . 94
.98
1.15
1.15
1.16
1.30
1.30
1.35
1.5,7
1.60
1.57
1.57
" 1.57
1.57
1.57
1.57
.75
.78
.90
.91
.98
1.08
1.18
.1*30
1.57
1.59
"" 1 . 89
1.70
1.76
1.70
"-' 1.70
1.59
1.34
PRESSURE
RENTIAL
H20I
ACTUAL
.94
.98
1.15
.1.15
1.16
1.30
'" '1.30
a. 35
••- 71.57
: 1.60
.1.57
. -rl'57
^1.57
4.57
Tl. 57
#1.57
''. .75
- .78
.90
.91
.98
1.08
1.18
= 1.30
1.57
1.59
"1.59
&•?£.
l.TO
1.70
1.70
1.39
: 1.34
.METER BOX NUMBER 6
METER HEAD DIFF. 1.85
C FACTOR 1.1
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS DIFF. 1.31
STACK
TEMP
(DEG.F)
90
90
90
90
90
90
94
93
94
95
95
95
95
94
94
94
94
94
94
93
95
97
97
97
"97
94
94
94
94
95
95
95
94
DRY GAS
METER
TEMP
(DEG.F)
INLET
80 "
83
85
90
94
97
- 101 -
104
106"
108
110
111
111
113
114
114
105
105
106
107
107
106
107
107
108"
108
108
108
108
108
108
108
104
OUTLET
80
80
80
81
83
84
86
88
89
91
93
94
94
96
"97
97
97
97
97
97
97
96
96
96
95
95
95
94
94
94
94
94
92
PUMP SAMPLE
VACUUM BOX TEMP
( IN.HG) (DEG.F !
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
.5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
5.0
5.0
5.0
5.0
5.3
5.5
5.5
""5.5
5.5
4.9
IMPINGER
TEMP
(DEG.F)
70" ~ ~
62
60
61
61
62
63
63
62
63
63
64
67
67
67
68
66
66
63
64
65
66
66
67
64
64
64
66
67
67
67
67
65
-------
PLANT . RALSTON PURINA..LOUISVILLE.KY. ' " "DATE u/06/72
SAMPLING LOCATION PELLET COOLER-INLET RUN NUMBER 1
DRY MOLECULAR WEIGHT DETERMINATION MOISTURE CONTENT DETERMINATION STACK GAS VELOCITY AND VOLUME DETERMINATION
GAS VOL. PERCENT IMP1NGER. MOISTURE.ML 16.0 STACK. AREA.SO. FT. 4.909
""" DRY BASIS SILICA MOISTURE.ML "24.2 PITOT TUBE COEFFICIENT " .85
—-» ' ' • - STACK ABS.PRESS, t IN.HG 29.49
C0~2 TOTAL MOISTURE.ML 40.2 STACK GAS TEM'PE'RATURE.DEG.F 9*
02 : STACK GAS MOL. WT.»WET BASIS 28.75.
"CO"" " " "" WATER VAPOR COLLECTED"." 1.905
N2 • -_ • __ST0» Cy. FT. _____
—--—" " "" " "SQRTfVELHD X STACK TEMP ABS) ~ " 22.9
TOTAL - GAS METER VQL..CU.FT.
GROSS TOTAL 88.374 STACK GAS VELOCITY, ACT. ffPS STTl
LESS LEAKAGE CORR . .000 STACK GAS VOLUME»STD CFM»
"DRY MOLECULAR" ~ "29.00 " — -; WET BASIS "15849.2
WEIQHT.LB/LB-MOLE NET TOTAL • 88.374 DRY BASIS 15494.5
DRY GAS VOL. THROUGH 83.246 ISOKlNETIC VARIATION
METER»STD. CU. FT —
_ __P|?CEN1 OF ISOKlNETIC SAMPLING 107.4
."MOISTURE CONTENT." " ".0224 " " " " " -----
VOL. FRACTION
i
I
-------
FIELD DATA
PLANT
SAMPLING LOCATION
. SA
OP
AM
BA
RALSTON
PELLET
MPLE TYPE PARTICU
ERATOR G FORTE
BIENT TEMP. (DEG.F) "60
R. PRESS. ( IN. HG) 29.58
PURINAi LOUISVILLE. (CV.
COOLER-OUTLET
LATE
STATIC PRESS! IN. M20) -.42
FILTER NUMBER! S) 200056
STACK INSIDE DIM(lN) 34.500
PITOT TUBE COEFF .85
READ AND RECORD DATA EVERY 3.
TRAVERSE
POINT
NO.
INIT
se-i
2
3
4
5
6
7
8
9
10
11
12
13
14
19
. 16
17
18
SW-1
2
3
4
5
-•,.-6
7 "
8
9
SAMPLE CLOCK
TIME TIME
(MIN.) (24-HR
~~ " CLOCK)
0 1340
"" 3.5
7.0
10.5
14.0
17.5
21.0
24.5
28.0
"31.5 "
35.0
38.5
42*0
43.5
49.0
52.5
56.0
59.5
63.0
66.5
70.0
" 73.5 "
77.0
80*5
84.0
87.5
91.0
94.5
GAS METER
READING
(CU.FT. )
605.400
607.010
608.600
610.180
6J1.690
613.660
615.460
617.280
619.170
621.110
623.040
625.000
626.790
628.690
630.560
632.520
634.530
636.480
638.332
640.110
641.860
643.600
645.410
647.290
649.180
651.140
653.130
655.180
5 MINUTES
VELOCITY
MEAD
JIN.H20)
.410
.430
.430
.500
• 510
• 540
• 550
.600
.630
.610
.570
.570
• 580
.610
• 630
.630
• 590
.610
.480
• 480
""" .490
.520
.570
.570
.620
.620
.670
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.H20)
DESIRED
. .44
.46
.46
.54
• 55
• 58
.59
.65
.67
.65
• 61
• 61
.62
.65
.67
.67
• 64
• 65
" .51
.51
.33
• 56
• 61
• 61
• 66
.66
" .72
ACTUAL
. .44
• 46
•- - .'46
.54
.55
.58
.59
.65
.67
.65
.61
.61
.62
.65
.67
.67
.64
.65
— - ,5l
.51
.33
.56
.61
.61
.66
.66
""" .72
DATE
R
- ---p
N
A
S
11/06/72
UN NUM3ES 2
ROBE LENGTH AND TYPE 3 FT GLASS
OZZLE I.D. .1875,
SSUMED MOISTURE. 2
AMPLE BOX NUMBER 0
METER BOX NUMBER 0
METER HEAD DIFF. 1.40 AT 0.75 SCFM
" C FACTOR 0.82
PROBE HEATER SETTING
HEATER BOX
REFERENCE
STACK
TEMP'
(DEG.F)
DRY GAS
TEMP
(DEG.
SETTING
PRESS DIFF. 1.78
METER
F)
PUMP SAMPLE
VACUUM BOX TEMP
(IN.HG) (DEG.F)
IMPINGER
TEMP
1 DEG.F)
INLET OUTLET
87
87
87
87
90
90
90
90
90"
90
90
90
"" " 90
9O
90
90
90
90
90
90
90
90
90
90
90
90
90
82
84
88
90
95
100
104
108
"112
115
118
120
122
124
126
128
128
129
126
126
127 "
128
128
128
129 -~
129
129 "
80
80
80
81
83
• 86
88
90
92
95
97
99
101
103
10.4
107
108
109
110
110
110 "
111
112,
112
""112"
112
~112
3.0
3.0
3.0
4.0
4.0
4.5
4.5
5.0
5.0
5.0
4.5
4.5
4.5
5.0
5.0
5.0
5.0
5.0
4.0
4.0
4.0
4.0
5.0
5.0
5.0
5.0
5.5
60
62
65
65
65
65
65
65
65
65
65
65
65
65
65
67
67
67
67
67
67
67
67
67
67
67
67
-------
PLANT
SAMPLING LOCAT ION
TRAVERSE
POINT
.NO.
10
11
12
13
14
15
16
17
18
TOTALS
AVERAGE
SAMPLE CLOCK
TIME TIME
(MIN.) (24-HR
CLOCK)
98.0
101.5
105.0
108.5
112.0
115.5
119.0
122.5
126.0 1546
126.0
RALSTON PURINA. LOUI SVI LLE »K V.
PELLET COOLER-OUTLET
GAS METER
READING
(CU.FT. )
657.190
659.170
661.150
663.150
665.220
667.310
669.430
671.540
671.657
66.257
VELOCITY
HEAD
(IN.H20)
.620
.620
.620
.630
.670
.680
.700
.700
.710
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.H20)
DESIRED
.66
.66
. .66
.67
.72
.73
.75
.75
.76
.62
ACTUAL
.66
.66
.66
.67
.72
.73
.75
.75
.76
.62
DATE
RUN NUMBER
STACK
TEMP
(DEG.F)
DRY GAS
TEMP
(DEG.
METER
F)
11/06/72
2
PUMP
VACUUM
I IN.HG)
SAMPLE IMPINGES
BOX TEMP TEMP
(DEG.F) (DEG.F)
INLET OUTLET
90
90
90
90
90
90
90
90
90
90
129
129
129
130
130
130
130
130
130
119
112
112
112
113
113
113
113
113
113
103
5.5
5.5
5.5
5.0
5.5
5.5
5.5
5.5
5.5
4.7
67
67
67
67
67
67
67
67
67
66
-------
PLANT
SAMPLING LOCAT
DRY MOLECULAR 'WEIGHT
__ GAS
C02
02
CO
N2
TOTAL
DRY MOLECULAR
WEIGHT, LB/LB-MOLE
RALSTON PURINA, LOUI SVILLE.KY.
ION PELLET COOLER-OUTLET
DETERMINATION MOISTURE CONTENT DETERMINATION
VOL. PERCENT IMPINGER MOISTURE, ML
DRY BASIS SILICA MOISTURE, ML
TOTAL MOISTURE, ML
WATER VAPOR COLLECTED,
STD» CU. FT.
GAS METER VOL.tCU.FT.
GROSS TOTAL
LESS LEAKAGE CORR
29.00 • — '
NET TOTAL
DRY GAS VOL. THROUGH
METER. STD. CU. FT
10.0
23.3
33.3
1.578
66.257
.000
66.257
60.863
DATE 11/06/72
RUN NUMBER 2
STACK GAS VELOCITY AND :VOLUNE
STACK AREA. SO. FT.
PITOT TUBE COEFFICIENT
STACK ABS. PRESS., IN. HG
STACK GAS TEMPERATURE, DEG.F
. STACK GAS MOL. WT..WET BASIS
SORTJVEL HD X STACK TEMP ABS)
STACK GAS VELOCITY, ACT. FPS
STACK GAS VOLUME. STD CFM,
WET BASIS
DRY BASIS
ISOKINETIC VARIATION
PERCENT OF ISOKINETIC SAMPLING
DETERMINATION
6.492
• 85
29.54
90
28.72
17.9
44*5
16501.7
16084,7
101.7
MOISTURE CONTENT*
VOL. FRACTION
• 0253
-------
FIELD DATA
PLANT
RALSTON PURlNAi LOUISVILL£»KY.
11/06/72
SAMPLING LOCATION
"SAMPLE TYPE ' ' '
OPERATOR
AMBIENT TEMP. (DEG.F)'
BAR.PRESS.tIN.HG)
PELLET COOLER-INLET
PARTICULATE"
R S AMICK
60
29.45
_DATE
RUN"NUMBER
PROBP LENGTH AND TYPE 4 FT GLASS
NO/.ZLE I.D. .1875
ASSUMED MOISTURE 2
SAMPLE BOX NUMBER 0
STATIC PRESS! IN.H20) -1.20
FILTER NUMBER)S) 200055
"STACK INSIDE DIMfIN)" 30.000
PITOT TUBE COEFF .85
READ AND RECORD DATA EVERY 4
MINUTES
METER BOX NUMBER
METER HEAD DIFF.
C FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS DIFF.
1.85 AT 0.75 SCFM
1.10
1.31
TRAVERSE
" "POINT ~~
NO.
SAMPLE
" TIME
(MIN. )
CLOCK
TIME
(24-HR
ri or* )
GAS METER
READING
(CU.FT. )
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H201 (
STACK
TEMP
DEG.F)
DRY GAS
TEMP
(DEG.
METER
F)
PUMP
VACUUM
( IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPINGER
TEMP
(DEG.F)
DESIRED ACTUAL
INLET OUTLET
INIT
N-l
• . 2
3__._
4
5
6
"7"
e
9
10
11
12
13
14
15
16
E-l
2
3
4
__5
6
7
e
9
10
- t 1
12
13
14
15
0
4.0
8.0
' ~12.0"
16.0
20.0
24.0
28.0
32.0
36.0
40.0
44.0
48.0
52.0
56.0
60.0
64.0
68.0
72.0
76.0
80.0
'84.0
88.0
92.0
96*0
100.0
104.0
108.0 "
112.0
116.0-
120.0
123.6
1625 245.908
248.094
250.354
"252.632
254.196
257.419
259.750
261.916
264.751
267.530
270.564
273.700
276.811
279.970
283.144
286*084
288*859
291.116
293.530
295,999
298.491
301.052
303.812
306.314
309*419
311.887
314.644
317.249
320*333
323*060
325.875
326.437
.570
.640
.640
.680
.720
.750
.800
.880
.980
1.200
1.200
1.200
1.200
1*200
1.200
.950
.650
.740
.760
.800
.880
.900
.950
.980
.980
1.000
1.000
1*000
1*000
1.000
1.000
.81
.88
.88
.95
.98
1.02
1.09
1.22
1.38
1.65
1.65
1.65
1.65
1.65
1.65
1.30
.91
.98
• 1.05
1.10
1.18
1.20
1.29
1.30
1.30
1.32
1.32
1.32
1.32
1.32
1.32
.81
.88
.88
.95
.98
1.02
1.09
1.22
1.38
1.65
1.65
1.65
1.65
1.65
1.65
1.30
.91
.98
1.05
1.10
1*18
1.20
1.29
1.30
1.30
1.32
1.32
1.32
1.32
1.32
1*32
96
96
96
94
95
97
96
94
90
90
90
90
90
90
90
90
90
90
90
92
: 92
92
90
90
90
90
90
90
90
90
90
82
88
91
94
96
97
V8
99
101
102
103
103
103
103
102
101
89
91
93
96
97
98
99
100
100
100
100
101
102
102
102
82
82
82
83
84
84
85
85
86
86
86
86
86
86
66
85
84
84
84
84
84
84
85
85
85
85
85
85
86
86
86
5.0
5.3
5.5
6.0
6.0
6.0
6.0
7.0
9.0
9.0
9.0
9.0
9.0
9.0
9.0
9.0
5.5
5.5
6.0
6.0
7.0
7.0
7.0
7.0
7.0
7.0
7.0
7.0
7.0
7.0
7.0
65
57
56 •"
56
57
57
57
57
57
57
57
57
58
58
58
.58
58
58
59
60
58
58
58
58
59
59
60
60
60
60
61
TOTALS
AVERAGE
123.6
82*529
1.25
1.25
92
65
7.1
58
-------
PLANT
SAMPLING LOCATION
RALSTON PURINA> LOUISVILLE.KY.
PELLET COOLER-INLET
DATE
RUN NUMBER
11/06/72
3
DRT-M?MC"LAJ? *ilG_!U_ DETERMINATION MOISTURE CONTENT DETERMINATION _ STACK GAS VELOCITY AND VOLUME DETERHINAT ION
GAS VOL. PERCENT IMPINGER MOISTURE.ML _ 18.0 S-TACK AREAtSO. FT. 4.909
DRY BASIS " SILICA MOISTURE.ML "16.6 P1TOT TUBE COEFFICIENT . . .85
j^ ^Z^^^l^l .STACK ABS.PRESS . . IN ._HG 29.36
C02 TOTAL MOISTURE«ML 34.6 STACK GAS fEMPERATURE.DEG.F 92
02 _ STACK GAS MOL. WT.tWET BASIS 28.77
CO " " - -.- . WATER VAPOR COLLECTED. '" 1.640
N2 __ ^ STD. CU. FT. _
------- " ~/~ SQRTIVEL HO X STACK TEMP ABS) 22.4
TOTAL GAS METER VQL.tCU.FT.
GROSS TOTAL 82.529 STACK GAS VELOCITY. ACT. FPS 55.9
•_ LESS LEAKAGE CORR _ .000 jSTACK GAS VOLUME.STD CFM.
DRY" MOLECULAR " "~ "29.00 -—:- ""' WET BASIS 15517.6
WEIGHTiLB/LB-MpLE _ NET TOTAL ;..._. 82.529 DRY BASIS 15199.5
. DRY GAS VOL. THROUGH 78.364 1SOKINETIC VARIATION
METER .STO. CU. FT —— -• —
_ . PERCENT. 0_F_ I SOU NET 1C SAMPLING _10'6.8
" MOISTURE CONTENT." "" .0205
VOL. FRACTION
-------
FIELD DATA
PLANT
<
<
c
"~ /
£
RALSTON
JAMPLlNG LOCATION PELLET
>AMPLE TYPE PARTICU
3PERATOR G FORTE
WBIENT TEMP. (DEO. Fi 50
5A.R. PRESS. ( IN. HG) 29.45
PURINAt LOUISVILLE»KY.
COOLER-OUTLET
.ATE
DATE
RUN NUMBE
PROBE LEN
NOZZLE I.
11/06/72
R 4
GTH AND TYPE 4 FT C
D. .250C
.LASS
'
ASSUMED MOISTURE 2
SAMPLE BOX NUMBER 0
STATIC PRESSIIN.H20) -.42
FILTER NUMBER! S) 200054
STACK INSIDE OIM(IN) 3*. 500 "
PITOT TUBE COEFF .85
METER BOX NUMBER
METER HEAD DIFF.
READ AND RECORD DATA EVERY 3.5 MINUTES
TRAVERSE SAMPL6
POINT " TIME
NO. (MIN.
INIT
SE-1
2
- 3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
16
"SW-1
2
.__ 3
4
5
6
7
8
" 9
0
3.5
7.0
10.5
14.0
17.5
21.0
24.5
28.0
"31.5
35.0
38.5
42.0
45.5
49.0
52.5
56.0
59.5
63.0
66.5
70.0
73.5
77.0
80.5
84.0
87.5
'91.0
94.5
--- - •.-
I CLOCK GAS METER
TIME READING
(24-HR (CU.FT.)
CLOCK)
1620 673.742
676.550
679.290
"682.090
685.010
688.180
690.890
694.570
697.930
701.300
704.650
707.990
711.290
714.620
718.160
721.710
725.250
728.720
732.093
" - - 735,320
738.540
" 741.840
745.410
748.470
752.010
755.320
758.760
762.110
- - - ------ - -
0
1.40 AT 0.75 SCFM
C FACTOR 0.82
PROBE HEATER SETTING .
HEATER BOX SETTING
REFERENCE PRESS DIFF. 1.78
VELOCITY ORIFICE PRESSURE STACK
HEAD DIFFERENTIAL TEMP
(IN.H20) (IN.H20) (DEG.F)
DESIRED
.430
.410
.430 ~~
.510
.540
.550
.570
.610
.640
.580
.600
.600
.620
.660
.680
.680
.650
.600
.540
.570
.580
.600
.620
.610
.610
.600
.590
1.43
1.35
1.43
1.70
1.80
1*82
1.89
2.00
2.10
1.92
1.93
1.98
2.02
2.18
2.20
2.20
2.15
1.98
1.80
1.89
1.92
1.98
2.02
2.00
2.00
1.98
1.95
ACTUAL
1.43
1.35
1.43
1.70
1.80
1.82
1.89
2.00
2.10
1.92
1.98
1.98
2.02
2*18
2.20 "
2.20
2.15
1.98
1.80
1.89
1.92
1.98
2.02
2.00
2.00
1.98
1.95
- - -
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM BOX TEMP TEMP
(DEG.F) (IN.HG) (DEG.F) iDEG.F)
INLET OUTLET
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
90
in*
.08
"" 108
110
115
120
122
126
128
130
131
132
133
134
135
136
136
136
132
131
131
132
134
134
135
135
135
95
95
95
95
96
98
99
100
102
1C4
104
105
107
108
108
109
110
110
110
110
no -""•
1.10
110
110
111
111
112
4.0
4.0
4.0
4.5
4.5
4.5
4.5
5.0
5.0
5.0
5.0
5.0
5.0
5.5
5.5
5.5
5.0
5.0
4,0
4.5
4.5
5.0
5.0.
5.0
5.0
5.0
4.5
82
82
82
82
84
84
84
84
84
78
78
72
72
70
66
65
65
65
63
63
"63 " "
63
65
65
65
65
65
-------
PLANT
SAMPLING LOCAT ION
TRAVERSE SAMPLE CLOCK
POINT '"TIME "TIME
NO. (MIN.) (24-HR
n net \
RALSTON PURINA* LOUI SVlLLE »KY.
PELLET COOLER-OUTLET
GAS METER VELOCITY ORIFICE PRESSURE
READING ~ HEAD DIFFERENTIAL
(CU.FT.) (IN.H20) (IN.H20)
DATE
RUN NUMSER
STACK DRY GAS METER
TEMP TEMP
(DEG.F) (DEG.F)
11/06/72
4
DESIRED ACTUAL
INLET OUTLET'
PUMP SAMPLE IMP-INGER
VACUUM BOX TEMP TEMP
(IN.HG) (DEG.F) (DEG.F)
10
11
12
13
14
15
16
17
16
98.0
101.5
105.0
108.5
112.0
115.5
119.0
122.5
126.0 1632
765.420
768.770
772.070
775.390
778.830
782.240
785.610
788.990
792.354
.580
.580
.580
.590
.600
.620
.630
• 600
.580
1.92
1.92
1.92
1.95
1.98
2.02
2.05
1.96
1.92
1.92
1.92
1.92
1.95
1.98
2.02
2.05
1.98
1.92
90
90
90
90
90
90
90
90
90
1351
~ 1351
136
136.'
136
136 .
136 '
136
136
"^
111!''''
1 1 ti fi !
112
112
lit
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
65
65
65
65
65
65
65
65
65
TOTALS
AVERAGE
126.0
116*612
1.93
1*93
90
130
107
4.7
71
-------
PLANT RALSTON PURINA. LOU I SVILLE »KY.
SAMPLING LOCATION PELLET COOLER-OUTLET
DRY MOLECULAR WEIGHT DETERMINATION
GAS VOL. PERCENT
DRY BASIS
C02
02
CO
N2
TOTAL
DRY MOLECULAR 29.00
WEIGHT.LB/LB-MOLE
MOISTURE CONTENT DETERMINATION
IMPINGER MOISTURE. ML
SILICA MOISTURE.ML
TOTAL MOISTUREfML
WATER VAPOR COLLECTED.'
STD. CU. FT.
GAS METER VOL..CU.FT.
GROSS TOTAL
LESS LEAKAGE CORR
NET TOTAL
DRY GAS VOL. THROUGH
METER»STD. CU. FT
12.0
33.6
45.6
2.161
118.612
.000
118.612
107.546
DATE 11/06/72
RUN NUMBER 4
STACK GAS. VELOCITY AND VOLUME DETERMINATION
STACK AREA.SQ. FT.
PITOT TUBE COEFFICIENT
STACK ABS. PRESS.. IN. HG
STACK GAS TEMPERATURE. DEG.F
STACK GAS MOL. WT..WET BASIS
SQRT(VEL HD X STACK TEMP ACS)
STACK GAS VELOCITY, ACT. FPS
STACK GAS VOLUME. STD CFM.
WET BASIS
DRY BASIS
ISOKINETIC VARIATION
PERCENT OF ISOKINETIC SAMPLING
6.492
.85
29.41
90
28.78
17.9
44.7
16493.6
16168.6
100.5
MOISTURE CONTENT*
VOL. FRACTION
.0197
-------
PLANT
SAMPLING LOCAT ION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP. (DEG.F)
BAR. PRESS. ( IN. HG)
RALSTON PURINA, LOUI SVILLE.KY.
PELLET COOLER-INLET
PARTICIPATE
R 5 AMICK
50
29.55
DATE
RUN NUMBER
PROBE LENG
NOZZLE I.D.
ASSUMED MO
SAMPLE BOX
STATIC PRESS.UN.H20) -1.55
FILTER NUMBER!S) 200060
STACK INSIDE DIM(IN)" 30.000
PITpT TUBE COEFF .85
READ AND RECORD DATA EVERY 4
MINUTES
11/06/72
.1875
2
_ _ 0
ME"TER"B'bX NUMBER 6
METER HEAD OIFF.
C FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS DIFF. 1.31
1.85 AT 0.75 SCFM
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
CLOCK)
GAS METER
READING
(CU.FT.I
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H20I
STACK
TEMP
(DEG.F)
DRY GAS
TEMP
(DEC.
METER
F)
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPINGER
TEMP
( DEC . F )
DESIRED ACTUAL
INLET OUTLET
INIT
E-l
2
3
4
5
6
7
8
9
10
11
12
13
14
" . " 15 '
16
N-l
2
3
4
5
6
7
e
9
10
...... u
12
13
14
15
16
0 1920
4.0
8*0
12.0
16*0
20.0
24.0
28.0
32.0
36*0
40.0
44.0
48.0
52.0
56.0
" 60.0 ~" r '
64.0 2024
68.0
72.0
76.0
80.0
84.0
8B.O
92.0
96.0
100.0
104.0
108.0"
112.0
116.0 7.
120.0
124.0
128.0 2140
328.627
331.124
333.454
335.860
338*299
340.821
343.341
345.921
348.600
351.050
353.674
356.111
358.962
361.664
364.271
366.944
369.673
372.108
374.217
~ 376.517
378.946
381*400
383.900
386*514
388*938
"391.584
394.296
396.500
399.673
"402.710
405.020
407.721
410.362
.680
.700
.750
• 820
.820
.820
.820
.850
.850
.870
.870
.880
.880
.910
.930
.950
.680
• 680
.630
.770
" .750
.770
.600
.820
.900
.930
.9.10
.910
.910
.910
.910
.860
.97
• 98
1.00
1.10
1.10
1.10
1.10
1.11
1.11
1.18
1.18
1.19
"1.19
1.20
1.28
1.30
.92
.92
.87
1.05
1.03
1.05
1.12
1.13
1.25
1.28
1.22
1.22
"""1.22
1.22
1.22
1.20
.97
.98
1*00
1.10
1.10
1.10
1.10
1.11
1.11
1.18
1.18
1.19
1.19
1.20
1.28
1.30
.92
.92
.87
1.05
1.03
1.05
1.12
1.13
1.25
1.28
1.22
1.22
1.22
1.22
1 . 22
1.20
90
90
90
92
92
92
93
92
91
90
91
90
90 "
90
90 —
90
90
90
90
90
90
90
90
90
"90
90
90
90
. 9Q ....
90
90
90
76
78
80
87
90
92
93
94
94
95
96
96
96
96
96
97
82
85
87
91
92
93
93
94
94
94
94
95 '
96
96
96
96
74
74
74
76
76
77
77
79
80
80
80
81
81
82
82
82
78
78
79
79
80
80
80
60
"81
81
81
*».•>
| 82 '•
92
-,!*•.
. 82
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.5
4.5
4.5
4.0
4.0 •
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4*0
4.O
4.0
4*0
4.0
4.0
60
60
58
60
61
61
60
60
60
60
60
61
62
63
65
65
65
65
65
66
66
66
60
61
61
62
63
63
64
64
64
68
"TOTALS
AVERAGE
128.0
81.735
1.13
1.13
90
92
79
4.0
62
-------
"PLANT "
SAMPLING LOCAT
DRY MOLECULAR WEIGHT
GAS
• •»•
C02
02
CO
N2
TOTAL
DRY MOLECULAR
WEIGHT. LB/LB-MOLE
:
RALSTON PURINA, LOUI SVILLE.KY.
ION PELLET COOLER-INLET
DETERMINATION MOISTURE CONTENT DETERMINATION
VOL. PERCENT IMPINGER MOISTURE. ML
DRY BASIS SILICA MOISTURE. ML
TOTAL MOISTURE.ML
WATER VAPOR COLLECTED,
_ STD. CU. FT.
GAS METER VOL..CU.FT.
GROSS TOTAL
LESS LEAKAGE CORR
29.00
NET TOTAL
DRY GAS VOL. THROUGH
METER.STD. CU. FT
MOISTURE CONTENT.
VOL. FRACTION
12.0
26.6
38.6
1.830
81.735
• 000
61.735
78.706
• 0227
DATE 11/06/72
RU.N NUMBER 5
STACK GAS VELOCITY AND VOLUME
STACK AREA. 50. FT.
P1TOT TUBE COEFFICIENT
STACK ABS. PRESS., IN. HG
STACK GAS TEMPERATURE. DEG.F
STACK GAS MOL. WT..WET BASIS
~SQRT(VEL HO X STACK TEMP ABS)
STACK GAS VELOCITY, ACT. FPS
STACK GAS VOLUME »STD CFM.
WET BASIS
DRY BASIS
ISOKINET1C VARIATION
PERCENT OF ISOKINETIC SAMPLING
DETERMINATION
4.909
.85
29.43
90
28.75
21.3
53.3
14875.9
14537.9
108.3
n
-------
FIELD DATA
PLANT
RALSTON
PURINA. LOUISVILLE.KY.
SAMPLING LOCATION PELLET COOLER-OUTLET
r~ SAMPLE TYPE ' PARTICIPATE .-
OPERATOR G FORTE
AMBIENT TEMP. (DEG.F I 50 -
BAR. PRESS. ( IN. HG) 29.40
STATIC PRESS) IN. H20) -.42
FILTER NUMBER! S) 200058
STACK INSIDE DIMUN) 34.500
PITOT TUBE COEFF .85
READ AND RECORD DATA EVERY 3.5 MINUTES
TRAVERSE
POINT
NO.
INIT
SE-1
2
3 ~
it
5
6
7
8
9
10
11
12
— i3-
14
15
16
17
16
" sw-i "
2
... - 3
4
*• 5
6
... . . 7-.^
6
"9 ""
SAMPLE CLOCK
TIME TIME
(WIN.) (24-HR
CLOCK)
0 1920
3.5
7.0
"10.5 "
14.0
17.5
21.0
24.5
28.0
'31.5 : "
35.0
38.5
42.0
45.5
49.0
52.5
56.0
59.5
63.0
66.5
70.0
" 73.5
77.0
80.5
84.0
67.5
91.0
94.5
GAS METER
READING
(CU.FT.)
793.144
795.940
798.710
801.560
804.530
807.610
810.750
813.980
817.320
820.730
824.160
827.480
830.840
834.280
837.770
841.490
844.990
.848.700
852.417
858.850
861.440
864.450
867.310
870*210
873.210
876.230
879.300
* 682.540
VELOCITY
HEAD
(IN.H20)
.440
.400
'.490
.490
.530
.540
"~ ~ .570
.610
.640
.620
.620
.630
.630
.640
.670
.710
.710
.740
.460
.460
.470
..470
• 460
• 460
.480
.500
.550
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H20!
DESIRED
1.45
1.35
1.62
1.62
1.75
1.80
1.89
2.00
" "2.10
2.05
2.05
2.08
2.08
2.10
2.20
2.35
2.35
2.40
1.55
1.55
1.56
1.56
1.55
1.55
1.60
1.65
1.82
ACTUAL
1.45"
. 1.35
1.62
1.62
1.75
1.80
1.89
2.00
2.10
2.05
2.05
2.08
"2.08
2.10
2.20
2.35
2.35
2.40
1.55
1.55
1.56
1.56
1.55
1.55
.1.60
1.65
1.82
-
STACK
TEMP
(DEG.F
90
90
~" 90
90
90
90
90
90
90
85
85
85
85
85
85
85
85
85
85
85
85
85
85
85
85
35
85
DATE
11/06/72
RUN NUMBER 6
PROBE LENGTH AND TYPE. 3 FT GLASS
NOZZLE I.D. .2500
ASSUMED MOISTURE 2
SAMPLE BOX NUMBER 0
METER BOX NUMBER 0
METER HEAD DIFF. 1.40 AT 0.75 SCFM
C FACTOR 0.82
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS DIFF.
DRY GAS METER
TEMP
I (DEG.F)
INLET
96
98
"102
106
110
114
116
119
120
123
124
126
127
128
129
130
130
131
128
129
130
128
126
124
125
125
126
OUTLET
94
94
94
92
92
92
93
95
96
98
98
loo
101
101
102
103
103
103
105
105
105
104
104
104
104
104
105
PUMP SAMPLE
VACUUM BOX TEMP
(IN.HG) (DEG.F)
4.0
4.0
4.0
4*0
4.0
4.0
4.5
5.0
5.0
5.0
5.0
5.0
5.0
5.0
.5.0
5.5
5.5
5.5
4.0
4.0
4.O
4.0
4.0
4.0
4.0
4.0
4.5
IMPINGER
TEMP
(DEG.F)
70
70
75
75
75
75
75
78
78
78
78
78
78
78
78 - -
78
78
80
80
80
80
80
80
77
77
77
77 :
-------
PLANT
SAMPLING LOCAT ION
TRAVERSE SAMPLE CLOCK
"POINT" TIME TIME"
NO. (MIN.I (24-HR
ri nrx \
RALSTON PURINA* LOUI SV iLLEtKV.
PELLET COOLER-OUTLET
GAS METER VELOCITY ORIFICE PRESSURE
READING HEAD ' " DIFFERENTIAL
(CU.FT.) UN.H20) UN.H20)
DATE
RUN NUMBER
STACK DRY GAS METER
"""TEMP TEMP
(DEG.F,
-------
PLANT
SAMPLING LOCAT
DRY MOLECULAR WEIGHT
GAS
C02
02
CO
N2
TOTAL
DRY MOLECULAR
WEIGHT.LB/LB-MOLE
RALSTON
ION PELLET
DETERMINATION
VOL. PERCENT
DRY BASIS
•«>—•—•-
29.00
PURINAi LOUISVILLE. ICY.
COOLER-OUTLET
MOISTURE CONTENT DETERMINATION
IMPINGER MOISTURE.ML
SILICA MOISTURE.ML
TOTAL MOISTURE.ML
WATER VAPOR COLLECTED.
STD. CU. FT.
GAS METER VOL.iCU.FT.
GROSS TOTAL
LESS LEAKAGE CORR
NET TOTAL
DRY GAS VOL. THROUGH
METEK.sTD. *.U. FT
MOISTURE CONTENT.
VOL. FRACTION
5.0
50.0
55.0
2.607
121.244
.000
121.244
110.894
.0230
DATE 11/06/72
RUN NUMBER 6
STACK GAS VELOCITY AND VOLUME
STACK AREAtSO. FT.
PITOT TUBE COEFFICIENT
STACK ABS. PRESS., IN. HG
STACK GAS TEMPERATURE. DEC. F
STACK GAS MOL. WT..WET BASIS
~SORT(VEL HD X STACK TEMP ASS J
STACK GAS VELOCITY. ACT. FPS
STACK GAS VOLUME. STO CFM.
WET BASIS
DRY BASIS
ISOKINETIC VARIATION
PERCENT OF ISOKINETIC SAMPLING
DETERMINATION _ _
6.492
.85
29.36
86
28.75
17.7 ""
44.3
"16436.1
16058.6
104.3
-------
FIELD DATA
PLANT
SAMPLING LOCATION
RALSTON PURINA, LOUISVILLE.KY.
HAMMERMILL OUTLET
DATE
RUN NUMBER
11/07/72
7
SAMPLE TYPE
" ~" "~ ""• OPERATOR
AMBIENT TEMP. (DEG.F)
"" ' " " BAR. PRESS. ( IN.HG)
.. STATIC PRESS1IN.H20)
FILTER NUMBER! S)
STACK INSIDE DIM! IN)
" PI TOT TUBE COEFF
PARTICULATE 1
R AMICK 1
60 '
29.20 :
-.31 1
200059 . " ' I
18.000 <
.85 1
READ AND RECORD DATA EVERY 7.5 MINUTES
PROBE LENGTH AND TYPE 24 INCH GLASS
NOZZLE I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER
WETER:~riEAD"T>rFFT~
FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS DIFF. 1.65
0.66
TKAVtKSE
POINT
NQ> _
SAMPLE
TIME
(KIN. )
CLOCK 5A5 MtTtH VELOCITY
TIME READING HEAD
(24-HR " (CU.FT.) (IN.H20)
CLOCK)
ORIFICE PRESSURE STACK DRY GAS MEltK MUMP SAMI^Lt
DIFFERENTIAL TEMP TEMP VACUUM BOX TEMP
(IN.H20) (DEG.F) (DEG.F) ( IN.HG) (DEG.F)
DESIRED
ACTUAL
iMHiftfcEK
TEMP
^DEG.F)
INLET OUTLET
INIT
N-l '
... . . . 2 ... .
3
4
5
6
7
" : e
w-l
"~ 2 "
3
4
5
. fc
7
-'8
TOTALS
AVERAGE
0
7.5
15.0
22.5
30.0
37.5
45.0
52.5
60.0
67.5
75.0
82.5
90.0
97.5
105.0
112.5
120.0
120.0
914.549
1230 92C.846
926.541
931.714
" 936.164
936.164
941.065
946.999
1330 " 954.495
1430 9.61.503
967.454 "
973.421
978.141
978.141
984.586
991.283
" 998 i 598 "
84*049
1.100
1.100
.970
.650
-.100
.700
1.600
1.600
1.400
1.200
1.200
.750
-.100
1.300
1.700
1.500
1.25
1.25
1.18
.75
.82
1.80
1.80
1.62
1.36
1.38
.87
— 1.48
1.95
1.68.
1.37
1
1
1
1
1
1
"" 1
1
1
..„. 1
1
.25
.25
.18
•75
.82
.80
.80
.62
.38
.38
.87
.48 "
.95
• 68
.37
70
70
70
J70
70
70
70
70
70
70
70
70.
70
80
80
80,
72
62
81
92
95 "
92
98
103
107
60
83
80
96
96
106
112
91
62
64
70
74
78
"80 '
80
83
60
64
69
76
76
80
85
73
3.0
3.0
3.0
3.0
.0
2.0
3.0
3.0.
4.0
3.0
3.0
3.0
.0
3.0
4.0
4.0 '
2.7
65
65
65
65
65
66
63
62
62
65
65
66
. 67
66
67
65
-------
PLANT
.SAMPLING LOCAT
DRY P.OLtCULAR WtltjHT
GAS
C02
02
CO
N2
TOTAL " ' -
DRY MOLECULAR
WEIGHT, LB/LB-MOLE
RALSTON PURINA, LOU I SVI LLE ,K Y.
ION HAMMERMILL OUTLET
DETERMINATION KolSTuRt CCNTtM "D'ETERM INAT ION
VOL. PERCENT IMPINGER MOISTURE, ML
DRY BASIS SILICA MOISTURE, ML
TOTAL MOISTURE, f-L
WATER VAPOR COLLECTED,
STD. CU. FT.
GAS. METER VOL..CU.FT.
GROSS TOTAL
LESS LEAKAGE CORR
29.00 ~
- • • • ""NET TOTAL
DRY GAS VOL. THROUGH
METER»STD. CU. FT
MOISTURE CONTENT,
-" ' VOL. FRACTION
.0
29.6
29.6
1.403
84.049
.000
84.049 "
80.471
.0171
DATE 11/07/72
RUN NUMBER 7
STACK' 'GAS VELOCI TY""AND VOLUMc Del
STACK AREA, SO. FT.
PITOT TUBE COEFFICIENT
STACK ABS. PRESS., IN. HG"
STACK GAS TEMPERATURE. DEC. F
"STACK GAS MOL. WT. .WET BASIS
SORTtVEL HD X STACK TEMP ABS)
STACK GAS VELOCITY, ACT. FPS
STACK GAS VOLUME, STD CFM ,
WET BASIS
DRY BASIS
ISOKINETIC VARIATION
'PERCENT OF ISOKINETIC SAMPLING
•FRMnsA-TTQI.
1.767
.85
29.17
72
26. SI
. 21.0
52.5
5408.8
5316.1
(111.3)*
116.2
. ...
Value computed when negative velocities are assumed to be zero
-------
.
— . ._
PLANT
SAMPLING LOCAT ION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP. (DEG.F)
BAR. PRESS. ( IN.HG)
STATIC PRESSIIN.H20)
FILTER NUMBER) S)
STACK INSIDE DIM(IN)
PI TOT TUBE COEFF
READ AND RECORD DATA
FJ
ELD DATA
RALSTON PURINA* LOUI SVILLE.KY.
HAMMERM ILL-OUTLET
PARTICULATE
R S AMICK
50
29.20
-.27
200061
18.000" "
.85
EVERY 4
DATE
RUN NUM
p?osr L
NOZZLE
ASSUMED
SAMPLE
11/07/72
3ER 8
iNGTH AND TYPE 24 FT
I.D. .1875
MOISTURE 2
30X NUMBER 0
METER BOX NUMBER
METER HEAD DIFF.
" C FACTOR
PROBE HEATER SETTING
MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
""POINT TIME "TIME READING HEAD
NO. (MIN.) (24-HR (CU.FT.I (IN.H20)
INIT
N-l
2
4
5
6
7
8
W-l
2
3
4
6
„. 7
8
V.LUV.KI
0 1620
4.0
8.0
12.0
16*0
20*0
24.0
28.0
32.0 1652
36*0
40.0
44*0
48*0
52.0
56.0
60.0
64.0 1700
998.866
2.380
5.724
8.654
10.673
12.544
13.614
19.085
21*862
26*544
30*085
33.361
35,999
35.999
40.454
44.321
48.652
1.400
1.400
.350
.410
.430
1.500
1*700
1.700
1.300
1.500
1*100
• 480
-. 100
1.300
1.750
1.800
-
0
1.40 AT 0.75 SCFM
0.86
1
1
HEATER BOX SETTING
REFERENCE PRESS DIFF. 1.65
ORIFICE PRESSURE STACK DRY GAS METER PUMP SAMPLE IMPINGER
DIFFERENTIAL TEMP TEMP VACUUM BOX TEMP TEMP
(IN.H20) (DEG.F) (DEG.F) (IN.HG) (DEG.F) (DEG.F)
DESIRED
1.60
1*60
" .41
.49
• 52
1.70
1.95
1.95
"1.52
1.70
1.27
.56
1.52
2.00
2.05
ACTUAL
1.60
1.60
.41
.49
.52
1.70
" 1.95
1.95
1.52
1.70
1.27
.56
1.52
2.00
2.05
80
80
80
80
80
80
80
80
76
76
76
77
76
76
""" 77
76
INLET
96
102
103
104
106
109
116
118
104
106
110
113
102
~ " 102
103
OUTLET
85
85
86"
87
88
88.
69
90
88
87
87
86
84
83
83
4.0
4.0
4.0
4.0
4.0
4.0
5.0
5.0
5.0
5.0
5.0
5.0
.0
6.0
7.0
7.0
60
61
60
60
60
60
60
60
62
63
64
65
65
65
65
u
1
M
TOTALS "
AVERAGE
64.0
49.786
1.39
1.39
78
106
86
4.6
62
-------
PLANT
SAMPLING LOCATION
RALSTON PURINA. LOUIiVlLLE.KYc
HAMMERMILL-OUTLET
DATE
RUN NUMBER
11/07/72
8
DRY MOLECULAR WEIGHT DETERMINATION MOISTURE CONTENT DETERMINATION STACK GAS VELOCITY AND VOLUME DETERMINATION •
• »»«»^«»»«»—»•••—«• — —• — »—*_« — ..•_. — •.*..« __.... «....._...._......._* — *_.>^-...__..___ — —— — -. — — — — —«. — -.-.•. — •.« — •»...• — .•—«..»•,.••»•» ....^^^ *
GAS VOL. PERCENT IMPINGER MOISTURE.ML .0 STACK AREA.SO. FT. 1.767 »'
DRY BASIS " SILICA MOISTURE.ML 15.1 PITOT TUBE COEFFICIENT , .85
—- — ——-— STACK ABS.PRESS. . IN.HG 29.18 "
C02 TOTAL MOJSTURE.ML 15.1 STACK GAS TEMPERATURE.DEG.F 78
02 __ _ STACK GAS MOL. WT..WET BASJS 28.83
CO' "" " "" " " " " WATER VAPOR COLLECTED. ' .716" — - -
N2 ______ _ STD. <-U. FT.
- - - ----- --- „......__--- - - . --- - SQRTtVEL HD X STACK TEMP ABS) 22.7
TOTAL •_ GAS METER VOL..CU.FT. ; •
GROSS TOTAL 49.786 STACK GAS VELOCITY. ACT. FPS 57.0
__ LESS LEAKAGE CORR .000 _ .STACK GAS VOLUME.STD CFM.
DRY MOLECULAR " 29.00 '"' ' — ~" " WET BASIS " 5800.5
WEIGHT»LB/LB*MOLE NET TOTAL _ .._>?.786 DRY BASIS 5712.5
. DRY GAS VOL. THROUGH 46.469 ISOKINETIC VARIATION (114.7)*
METER.STD. CU. FT ~
. PERCENT. OF ISOKINETIC SAMPLING 117.1
•~ " '". "" "MOISTURE CONTENT. "" ".0152
'_ . VOL. FRACTION _
. • " • • ~ .•"•"" " - — -
w
• w
. • . - I
?
, -' ' ' - ,n_u:__ . -- -- '— -T-— _._-_.__ - • f.- —. r _... - —- - _...-. -..--- -1 ---^ C
'JL".'".V -I ".' .''_"--"'.'"' '"** . - -'!."--'.-•'-' •• • ' .'••• _ -,.„.. '. _ „ • ;^ _ .. . ... '. . . -
Value computed when negative velocities are assumed to be zero
-------
PLANT
SAMPLING LOCATION
" SAMPLE TYPE "
OPERATOR
AMBIENT TEMP.I DEG.F)
BAR. PRESS. (IN. HO)
STATIC PRESSIIN.H20)
FILTER NUMBER) S)
STACK INSIDE DIM(IN)
PI TOT TUBE COEFF
READ AND RECORD DATA
TRAVERSE SAMPLE CLOCK
POINT TIME "~ TIME
NO.
-------
PLANT
SAMPLING LOCATION
RALSTON PURINA, LOUISVILLE. KY.
HAHMERMILL OUTLET
DATE
RUN NUMBER
11/07/72
9
DRY MOLECULAR WEIGHT DETERMINATION MOISTURE CONTENT DETERMINATION STACK GAS VELOCITY AND VOLUME DETERMINATION
G«S _ VOL. PERCENT . IMPINGER MOISTURE.ML .0 STACK AREA.SO. FT. 1.767
" DRY BASIS SILICA MOISTURE,ML 19.1 PI TOT TUBE COEFFICIENT ' .85
—- . ————•—- -~— STACK ABS.PRESS..IN.HG ' 29.13
C02 TOTAL MOISTURE.ML 19.i STACK GAS TEMPERATURE.DEG..F 76
02 STACK GAS MOL. WT..WET BASIS 28.81
CO "" ~: " WATER VAPOR COLLECTED."" .905
N2 STD« CU. FT.
" "" ——— SORTJVEL HD X STACK TEMP ABS) 2^.8..
TOTAL GAS METER VOL.nU.FT.
GROSS TOTAL 51.758 STACK GAS VELOCITY, ACT. FPS 62.1
LEbb LEAKAGE CORR .000_ STACK GAS VOLUME,STD CFM,
"DRY MOLECULAR" " ~" 29.00 " " '• "" WET BASIS " 6352.3
WEIGHT.LB/LB-MOLE NET TOTAL 51.758 DRY BASIS 6240.3
DRY GAS VOL. THROUGH 50.419 1SOKINET1C VARIATION (114.1)*
METER»STD. CU. FT f —
_ _ _J _ PERCENT OF ISOKINETIC SAMPLING 116.3
r "" MOISTURE CONTENT, ~ .0176
•- • y9J^__!i5A!-!!ON_ _.__ ..:
t »-._i_ri_..T.- : - .----- I- ' -i r- -I — •- - -.-,-.. - - - —. --'- J .*
- • ' •' '
„_ . * r ' " ~ " ~ ' "-"'--•' -- - • - - - ..... . — .
Value computed when negative velocities are assumed to be zero
-------
PLANT_
DATE
SAMPLING LOCAT'Oti
SAT.PLE TYPE
RUN NUMBER
OPERATOR
ft/IS./IV A
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE 3-
STATIC PRESSURE,
FILTER NUMBER(s)
STACK DIMEN. 3G -i,, t.
PITOT TUBE "£" -ryr
-------
FI
PLANT
DATE_J
S/VIPLI N'G" LOCAT1 ON"
SAMPLE TYPE
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE, (Ps)
FILTER NUMBER(s) ~_
STACK DIHEN.
PITOT TUBE
TA
PROOF. LF:;GTH ADD TYPE_
NOZZLE I.D._
ASSUMED MOISTURE, J_
SAMPLE BOX NUMbER;
METER BOX NUMBER
METER iHn
C FACTOR
PR03E HEATER SETTING
HEATER BOX SETTING
REFERENCE 6p
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY
-44
7 8 9 10
TRAVERSE
POINT
NUMBER
"1.
%
a
fa
il
ll.
13
i4
l<5
\fa
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11
12 13 14J15 16 1718
^SICLOCK TIME
TIM£,min ^^CLOCK)
0
52..
£\
1,
((
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1
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1 I(p9
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124-t
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9
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9
0
0
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0
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0
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1536
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1920 2 1 22 23 24
GAS METER READING
(VJ, ft3
,
2. \1 .4 2.4
tG^
4- 1
2,2.^ , 1 2. 1
)
-2-3 £„ 231
^35" e^0!^
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2526 272829
VELOCITY
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3031 32 33)3435 3637
ORIFICE PRESSURE
DIFFERENTIAL
(AH) .in.HjO)
DESI.RED
.115
o3
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1 0 t{ ?
leSH
e
o
9
9
O
9
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ACTUAL
1 9 • O
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1.57
1,5^
|oSC
,~7(
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£
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>
QS
cf 5
i i
42 43 44 |45 46 4 7
DRY GAS METER
TEMPERATURE
INLET
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id
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OUTLET
mout '
'9 <^
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484950 51
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in.Hg
>4- j *
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5" «t i
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£~4>
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SAMPLE BOX
TEMPERATURE
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55 56 57
IMPINGER
TEMPERATURE
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7
67
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LEAKAGE
_'Hg -
GAS METER COR.
CFM
78 9 lOM
PEDCo - ENVIRONMENTAL.
SUITE O • ATKINSON SQUARE
CINCINNATI. OHIO A5ZAB
-------
Fia
PLANT
DATE
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER_
OPERATOR
7<_t r
PROBE LK:;GTH A:JD TYPE
NOZZLE I.D. d I 0
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE, (P
FILTER NUMBER(s)
STACK DIMEN.
PITOT TUBE
ASS.UMED MOISTURE, \
SAMPLE BOX NUMBER "
MUTER BOX NUMDER ~
METER flHg / , 4-ZTjg
C FACTOR (O'eZl
Q ,
-
PROBE HEATER SETTING
HEATER BOX SETTING ~
REFERENCE Ap
rype
SCHEMATIC OF TRAVERSE POIHT LAYOUT
READ AND RECORD ALL DATA EVERY 3 e5" MINUTES
7 8 9 10
11 12 13 14J15 16 1718
1920 21 22 23 24
2526 2728 29J30 31 3233J3435 3637
38 39 40 41
42 43 44 |45 46 4 7
484950 51
52 53 54
55 56 57
TRAVERSE
POINT
NUMBER.
CLOCK TIME
SAMPLINGS. (24 hr
TUtf^min \CLOCK)
GAS METER READING
(vm) , ft3
VELOCITY
HEAD
(Ap8) ,in.H20
ORIFICE PRESSURE
DIFFERENTIAL
(AH) ,in.H2O)
STACK
TEMPERATURE
(T),°F
DRY GAS METER
TEMPERATURE
INLET
6*9,5 • 4-OO
DESIRED ACTUAL
OUTLET
out
. PUMP
VACUUM,
in.Hg
IMPINGER
TEMPERATURE
•F
07
82-
8 o
3.0
7.0
g?
84-
.43
3.°
s-f
67
90
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4,0
65"
95-
83
.ft
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It
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lot
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67
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5.0
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sW-
1L
lio.
_fc7_
7(7.
-------
PLANT
DATE
S ;•_••: P LI NG LOCATI ON
SAMPLE TYPE
RUN NUMBER
OPERATOR
-3=
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE, (Pg)
FILTER NUMBER(s) "
STACK DIMEN.
PITOT TUBE
-EJE
PF.OI.'E LKNGTH AND TYPE
NO.-'ZLE I .D.
FAvi'i.E BOX NI;MBER_
r.LTCR ROX NUMBER_^
KE-TER iHg
C FACTOR
PP03E HEATKR SETTING
HEATER BOX SETTING ~
REFERENCE 6p
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AJiD RECORD ALL DATA EVER* 9 MINUTES
pZ-
8 9 10
TRAVERSE
POINT
:S. CLOCK TIME
SAMPLINGS. (24 hr
TIKE,min X.CLOCK)
0
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45 46 47
DRY GAS METER
TEMPERATURE
INLET
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130
130
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OUTLET
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out
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5~,7
67
67
II
LEAKAGE
GAS METER COR.
CFM
789 10 U
PEDCo - ENVIRONMENTAL.
SUITE O • A T K I N to O N SQUARE
CINCINNATI. <"yl-)IO 1524S
-------
FIELD DATA
SAMPLE TYPE
RUN NUMBER
rEMPE
OPERATOR_
AMBIENT TEMPERATUF
DAKOMETRIC PRESSURE"
STATIC PRESSURE, (P~
FILTER NUMBER{s)
STACK DIMEN.
PITOT TUBE
QOO
r;;oi^
52
^S
-72.,
76.
£3L
J 1—I °ll' . ' I | i o i ' '
1 1
I.F.AXAGE 8
GAS METER COR.
CFM
78 9 10 11
PEDCo - ENVIRONMENTAL.
SUITE B • ATKINSON SQUARE
CINCINNATI. (TMIO AS2AO
-------
FIELD DATA
SAMPLING LOCATION
SAMPLE TYPE J ~_
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE,
STATIC PRESSURE, (Ps)
FILTER NUMBER (s) ]
STACK DIMEN.
PITOT TUBE
PRO! r LFNGTII ;.ND TVPE_
NO"L1.E I.D.
A^SL •••.cu MOISTURE", %
S,Vi I.E BOX NU.-'.UER
MI.Ti R BOX NUMBER
METER AHp
C
_
PROHE HEATER SETTING
HEATER BOX SETTING ~
REFERENCE ip
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY 4f~ B> MINUTES
8 9 10
11 12 13 14|l5 16 1718
1920 21 22 23 24
2526 2728 29J30 31 3233|3435 3637
38 39 40 41
424344|45 46 47
484950 51
52 53 54
55 56 57
rRAVERSB
POINT
NUMBER
CLOCK TIME
SAMPLINGv (24 hr
TIHE,min
GAS METER READING
4>b_ ."&_/
- "ft "^ ""^r~~,m
7TH
t .
^
J^
/
JL
~S 7
I i « i 1
-1—L
! _ L
1 l-
1 . 1
CAS METER COR.
CFM
78 9 lOH
PEDCo - ENVIRONMENTAL
SUITE G • ATKINSON SQUARE
Cir-JCINNATI. OHIO 4S24S
-------
PLANT_
DATE
SAMPLING LOCATION
SAMPLE TYPE fA^Tl
RUN NUMBER ~f
OPERATOR
72-
Pei
£g-- £>U~UST~
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE'
STATIC PRESSURE, (P]
FILTER NUMBER (s) '
STACK DIMEN.
PITOT TUBE
PROUr LENGTH AND TYPE
NOZZLE I.D.
ASSUMED MOISTURE, %
SAMPLE BOX NUMUER_
MUTER BOX NUMBER
METER AHg
C FACTOR
Q.&2-
0-~IT
PROBE HEATER SETTING -_
HEATER BOX SETTING —
REFERENCE 6p ^
SCHEMATIC OF TRAVERSE POIHT LAYOUT
READ AND RECORD ALL DATA EVERY 3
7 8 9 10
11 12 13 14J15 16 1718
1920 21 2223 24
2526 272829
3031 32 33)3435 3637
38 39 40 41
4243 44|45 46 4 7
484950 51
52 5 3 54
55 56 57
TRAVERSE
POINT
NUMBER
TlME,min
TIME
(24 hr
GAS METER READING
, ft3
VELOCITY
HEAD
o
I0*#
.43.
/ A-3
20-
6
4
I+.O
1*70
Uo-
6 2-
It*
6 4
\-Z-0
e 4
. 57
8
c 33
z.gg
1&Q.
$0
5,0
70/
64-
2U/O
$0
102.
10
ar.o
704-
.S6
104
/I
1.96
$0
104-
S'aO
•/£-
&_Q__
l os-
_&l_
JOJ_
Z*!®
J3±
10ft
£".£
_zc_
AT
issr
Lie
/(=
68
I3b
10°)
il
-8 7Z,
(05
/S
2>0
tlo
/B
1(0,
135.
2>0
$0
132^
no
13 /
d*£
{,3
•736-5-
14-1
JLQ-
A*5.
-f
77.0
£>£>
II- 0
1 0 I
i '
I
LEAJIAGE 9 1-iT '»g -
GAS M1JTLR COR. C?
PEDCo - ENVIRONMENTAL
SUITE 8 • ATKINSON SQUARE
CINCINNATI. OHIO A
7 8 9. 10M
-------
PLANT
DATE
SAMPLING LOCATION fli/TCer
SAMPLE TYPE M
RUN NUMBER
J^L
OPERATOR T
AMBIENT TEMPERATURE
BAROMETRIC
PRESSURE
STATIC PRESSURE, (P_)
FILTER NUMBER (s)
PROBE LENGTH AND
NOZZLE I.D.
ASSUMED MOISTURL
TYPE
%
SAMPLE DOX NUMBER
METER BOX NUMBER
METER A
HB
C FACTOR
PROBE HEATER SETTING
HEATL'R BOX SETTING
REFERENCE Ap
STACK DIMEN.
7 8 9 10
TRAVERSE
POINT
NUMBER
SM/-S-
6»
7
&
*>
10
n
it-
13,
M-
ir
l(o
17
/e
L JU I,, '
11 12 13 14
PITOT TUBE
15 16 1718
\. CLOCK TIME
SAMPLINGS. (24 hr
TIME,min ^^CLOCK)
0
e>o»s~
0T* O
87, 5-
^/o 0
94-,r
e>£9C>
)Ol»S~
10?* 0
;?>
7°>2~ 92>&4-
9
e
o
0
e
• ' e
8
a -
0
1 ! Oil
SCHEMATIC OF TRAVERSE POIHT LAYOUT
READ AND RECORD ALL DATA EVERY _a2_S_5INUT
2526272829*3031 3233]3435 363738 39 40 41
VELOCITY
HEAD
(Ap ) , in.H O
s «
o*&z.
ofal
ofal
*(oO
„ £"<£>
• 5®
• s€>
„ £&
9 5~^>
c (0O
•Q \& O
0 T&
o
o
o
0
0
o
o
o
1 Oil
ORIFICE PRESSURE
DIFFERENTIAL
(AH) ,in.H2O)
DESIRED
2^,0-i.
2^o0
2o 00
I <>3£
19^S
l*?>2-
1 • 92.
I o <2>z-
|0$>5'
|.3>g
i^o-z.
2^os~
\**>&
(9?>2-
a
0
e
o
0
0
0
o
o
1 0 1
ACTUAL
- Z-0<92-
~i*&&
2*oo
I o36
(0^S
/.9Z-
/ e^ 2-
( 09Z.
/o^'
i ^ 0
-2V02.
2«£\y
/ Oj^l
/ &\ -?
e
o
o
e
0
0
e
c
c
1 0 1
STACK
TEMPERATURE
CT8),'F
85 &
t>0
°>o
0)0
^O
0,0
^o
. <*) O
tyo
Q) Q
*$£>
^^/^
°)0
1 1 1
ES
424344|45 46 47
DRY GAS METER
TEMPERATURE
INLET
(T ) , °F
mtn
l^>^
134-
(3S'
I35~
155'
/3J—
t^S"
\bb
O<*
l~$(o
1 ~Zo
4.s5"
^iT
T*J"
-4i5"
%5"
•^•5"
^5
4«
-------
FIELD DATA
DATE
LOCATION
SAMPLE TYPE
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE
DAROMETRIC PRESSURE
STATIC PRESSURE, (P
FILTER NUMBER(s)
STACK DIMEN.
PITOT TUBE
FKO!-r LKNGTH AN'D TYPE
.•.•O"r.!.E I .D.
F.Vi-LF. POX NUMBER
H! TfR i!OX NUMBER_
METER 6Hg ^
C FACTOR
PP03E HEATER SETTING
HEATER BOX SETTING
REFERENCE Ap
x.-
? 8 9 10
11 12 13 14J15 16 1718
1920 21 2223 24
SCHEMATIC OF TRAVERSE POINT LAYQUT
READ AMD RECORD ALL DATA EVERY
2526272829,3031 3233J3435 3637
38 39 40 41
424344)45 46 47
484950 51
52 53 54
55 56 57
TRAVERSE
POINT
NUMBER
SAMPLIN(
TIME,min
TIME
(24 hr
CLOCK)
GAS METER READING
(VJ, ft3
(4ps),in.H20
ORIFICE PRESSURE
DIFFERENTIAL
(6H) ,in.H20)
STACK
TEMPERATURE
(T ),'F
DRY GAS METER
TEMPERATURE
INLET
DESIRED
ACTUAL
OUTLET
(Tm ) ,
mout
. PUMP
VACUUM,
in.Hg
SAMPLE BOX
TEMPERATURE
•F
IMPINGER
TEMPERATURE
•F
^3 t . \ Z4
i£Z
333
335.
a*.
^m
Ml
(/
A/
78
~3~14-. £ /
92
L
374, si 7
^n*i
6
101
' P I I
i » 1 1
i °
II
,1
LEAKAGE g \^ 'Hg - O ^ CFM
GAS METER COR.
PEDCo - ENVIRONMENTAL-
suiTE O • ATKINBON SQUARE
CINCINNATI. OHIO
-------
PLANT
DATE_
SA-MPLfNG LOCATION
SAMPLE TYPE ~
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE
DAROMETRIC PRESSURE
STATIC PRESSURE, (Ps)
FILTER NUMBER(s) ~
STACK DIMEN.
PITOT TUBE
FIELD DATA
PRO!:." LKNGTH AfiD TYPE
NO::
A;-G
:LE i .D.
"•.ED MOISTURE, %
•LE BOX NUMBER ~
~.K BOX NUMBER
KETER iHp
C FACTOR
PP.C3E HEATER SETTING
HEATER BOX SETTING ~
REFERENCE Ap
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD AH. DATA EVERY ^+ 8W1INUTES
9 10
11 12 13 14|l5 16 17 18 1920 21 22 23 24
2526272829(3031 3233J3435 3637
38 39 40 41
4243 44|45 46 4 7
484950 51
52 53 54
55 56 57
CLOCK TIME
SAKPLINGV. (24 hr
TIHE,min
GAS METER READING
(v>, ft3
VELOCITY
HEAD
(ips),in.H20
ORIFICE PRESSURE
DIFFERENTIAL
(6H) ,in.H.,0)
STACK
TEMPERATURE
(T ),"F
DRY GAS METER
TEMPERATURE
DESIRED
ACTUAL
IHLET
in
OUTLET
(T ) ,
mout
. PUMP
VACUUM,
in.Hg
SAMPLE BOX
TEMPERATURE
•f
IMPINGER
TEMPERATURE
•F
1JZ
J*JZ
T3K
/,/3
JU-
Z-
-t*42r
1.22-
1.22.
1. 22.
L22.
jo"
psy
rz
I - 1 - a _ i
I ° I
1 01
1 1
_ 1
J-E71KAGE
•Hg - : CFM
GAS METER COR.
789 ion
PEDCo. - ENVIRONMENTAL-
suiTE O • ATKINSON SQUARE
CINCINNATI. OHIO •O5248
-------
1.A7A
PLANT
DATE 6 A/gV'
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER_
OPERATOR
7 2-
_gT CCOL~£K.~ C*_>r<_£T
flg-T I Ct/W? T£" & _
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE, (P
FILTER NUMBER(s)
STACK DIMEN. _
PITOT TUBE
••s"
"vTi
PROBE LJ':;CTII A;;U TYPE ~S '
NOZZLE I.D. Q . 2S" Q
ASSUMED MOISTURE, % -g_
SAMPLE BOX NUMLiER —
MLTER BOX NUMBER_ —
ME-TER £Hn
C FACTOR
4o
PROBE HEATER SETTING —
HEATER BOX SETTING -
REFERENCE flp -
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY 3 aS"MINUTES
7 8 9 10
14|l5 16 1718)192021 222324
2526272829*3031 3233]3435 3637
38 39 40 41
4243 44 |45 46 4 7
484950 51
52 53 54
55 56 57
TRAVERSE
POINT
NUMBER
. CLOCK TIME
SAMPLING >v (24 hr
TIME,min \CLOCK)
GAS METER READING
+-
JO* ff
-f-/?
4-
7r
n.s
/oTT
no
U2
75
4*0
7
0/3 . <>>£>
(a
7.T-
20.0
617
l/l
3/cJT
Of"
12-0
S.O
70
/o
70
II
loo
13
45-^
0%
101
•78
4°>>0
77
10
76
If
f •>
67
/it
"71
35"
76
11
(6
O
74
131
SU/~ (
05
/OS"
.66
/•sr
42.
77.
2±
±L
i-zb
-J&
j—i—i—° i i i i i
1 o 1
1. _ !
1
LEAKAGE ? /5~*Hg - Q CFM
GAS ;4ET'L;R COR. £ .
PEDCo - ENVIRONMENTAL
SUITE 6 • A.TKINSON SQUARE
C-INCINNATI. OHIO 4
78 910H
-------
n
TA
PLANT_
DATE "^_
SAMPLING LOCATION
SAMPLE TYPE "
RUN NUMBER & £,
OPERATOR
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE,
FILTER NUMBER (s)
STACK DIMEN.
PITOT TUBE
_
(Ps)
~
PROBE LENGTH Ar.'D TYPE
NOZZLE I.D. ~
ASSUMED MOISTURE, i
SAMPLE BOX NUMBER
METER BOX NUMBER
ME-TER AHg
C FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING ~
REFERENCE 6p_
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY ?, p.^MINUTES
7 8 9 10
11 12 13 14J15 16 1718
19 20 21 22 23 24
25 26 2728 29J30 31 32 33J34 35 36 37
38 39 40 41
424344)45 46 47
484950 51
52 53 54
55 56 57
TRAVERSE
POINT
NUMBER
. CLOCK TIME
SAMPLINGS. (24 hr
TIME,min \CLOCK)
GAS METER READING
<« ffc3
VELOCITY
HEAD
ORIFICE PRESSURE
DIFFERENTIAL
(AH) .in.HO)
STACK
TEMPERATURE
DRY GAS METER
TEMPERATURE
DESIRED
ACTUAL
INLET
(Tm ) ,
OUTLET.
(Tm ) ,
out
. PUMP
VACUUM,
in.Hg
IMPINGER
TEMPERATURE
•F
$-70 .
#5-
46
77
876? .
73-5-
77
„ 5-Q
1 o
/.^r
J&.
77
$4-
/asr
77
If)
/Z.7
tar-
77
II
IDI.S
Z./9Z,
5-.C
7-?
10$-*
&5T
/ol-
77
15
32
63
2^/0
$5-
131
77
ill*o
77
732,
g
Z+Z&
lo~7
77]
n
fir
7
•77
10,
S___J_L
IQI
i _ i
LEAKAGE 8 "fig - CFM
GAS METLR COR.
PEDCo - ENVIRONMENTAL.
SUITt; O • ATKINSON SQUARE
CIN Cl N N ATI. OHIO 45246
78 9 IOH
-------
PLANT
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE
BAROMETRIC'PRESSURE
STATIC PRESSURE, (P
FILTER NUMBER(s)
STACK DIMEN. /
PITOT TUBE rc=r-r
Til AND TYPE
, / o 75
[
ft
VELOCITY
HEAD
(ip8),in.H20
ORIFICE PRESSURE
DIFFERENTIAL
<&H) ,in.H20)
STACK
TEMPERATURE
(T8),'F
DRY GAS METER
TEMPERATURE
INLET
DESIRED
ACTUAL
OUTLET
out
. PUMP
VACUUM,
in. Kg
SAMPLE BOX
TEMPERATURE
•F
IMPINGER
TEMPERATURE
•F
N- /
U7-5
1.15
70
0,21
^ .0
.nTT
\.\
-k
•?*
3SE
uA.
^^
.()
/ I
_x
7o
.(}
ii
635
t$-7
3 • 42. J
4ftil
gqr-.
,).,.!
J L
JL
_L
LEAKAGE 9 \^ "Kg - Q. CFM '
GAS METER COR.
e ^x^
7 81 9MO 11
a^
r3 - ^^<
PEDCo - ENVtRONMENTAL-
__SUITE O ' ATKINSON SQUARE
_, I] , .•» 1 ICiNCINNATI. OHIO4524G
Stt*3iji^jfciwdis«t*«*'. ' a /
_--*
-------
IATA
PLANT
SAMPLING LOCTTION
SAMPLE TYPE
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE _ ,.
STATIC PRESSURE, (P5 ) - «•
FILTER NUMBER(s) "
STACK DIHEN. \9 >"rx
PITOT TUBE lv<"
AND TYP
. /$
PRObE LF.'.'GTii
NOZZLE I.D.
ASSU'-tED MOISTlPL, »
SA-'-'.PLE BOX NL:XbER
METER BOX NUHDER_"
ME-TER iHa
C FACTOR^"
7
PRO3E HEA7KRSETTTNG
HEATER BOX SETTING '_
REFERENCE flp £ ^
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY p MINUTES
LEAKAGE ? 'Bg - (O.CTH
•*" »•"---« r •;-• ^F— —
GAS METER COR
•—4-4—
7 «9 10 11
PEDCo - ENVIRONMETNTAL
SUITE O • ATKIMSON SQUARE
CINCINNATI. OHIO ^D21O
-------
PLANT
SAMPLING £OCATION
SAMPLE TYPE P?
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE 5
BAROMETRIC PRESSURE
STATIC PRESSURE,
FILTER NUM&ER(s)
STACK DIMEN.
PITOT TUBE
PROUE LF;:GTH ;>:;D TYPE J 4-
NOZZLE - - "*-" ^ "•'•
ASSU'-'.EI
SA.",PLE BOX NUMbER
MLTER BOX NUMBER.
ME-TER ,
C FACTOR^
PROBE HEATER STiTtlNG
HEATER BOX SETTING
REFERENCE fip
"
SCHEHATIC OF TRAVERSE POINT iAYOBT
READ AND RECORD ALL DATA EVERY ^j„ tluNUTES
55 56 57
LEAKAGE g 15 "Hg - (0 CFM
GAS MUTLU COR. (j) . A)
7~^ 9 1 0 1"
PEDCo - ENVIRONMENTAL
SUITE a • ATKINSON! .SQUARE
CINCINNATI. OHIO 45246
-------
GAS VELOCITY AND VOLUME DATA
VELOCITY TRAVERSE DATA
Point
tf-/
;Z,
.3
4.
'c
^
r^
A
y
/O
//
jj~
/3
/4~
/S
£*-/
^2
^
-^
7
Position
Inches3
/,£>&
/,
Total
Average
Reading, Ap
>?.^f 5
.^52.
,6"5"
,c?e
.70
.73
.77
.€>4
,e>/
,32-
.t>2.
,»>Z;
• 5/
.09
^0C»
,7&
O-54-
,b4-
,(o&
,17
,7$
• Bo
,^3
- •
-
^
T °F
s
^o
.
Test No . 7 t/W: TT^Uc.^^
Location ~7^/4&7 &e>4e^'
Stack Inside Dimensions 3C1' <^5 (jS/i* uippue.} "^"^
Stack Area, A_ = sq. ft.
E)
Stack Gage Pressure = — /.fc "H-0
C4-=iy-^V A He T> >*o c c 11 i-o O — "UiH .1. D fl H.
13.6 b
C+-1a/-»L' Pao T*£imr-v T*— OpA^CA On
Molecular Weight of Stack Gas, M =
/ — • ' r • s • •
— 174 V/A?-> fn \/T v ")Q Q9 v 9Q' •P^/min
— j. / 4 y iip v_p y i c x ^y.y/ x ^;7 rt/iuin.
8 P M
s s
Vs =
Q, Volume = ft/min. x sq . f t . = cfi
f oudnuctia vuj.ume cit. /u r anu ^:/i j^: rly (W6t J33.S1SJ —
v»
Q x 530 x Ps = 17.7 x x =
T 29.^92
. S
Q_ - Q,, x (100-W)/100 -
/ £ *
a) From outside of port to sampling point. ( /
Pi tot tube
-------
GAS VELOCITY AND VOLUME DATA
VELOCITY TRAVERSE DATA
Point
fr
-------
-GAS VELOCITY AND VOLUME DATA
VELOCITY TRAVERSE DATA
Point
-5- /
•2,
J?
«^1
7,
ft
*9
JfO
//
/2,
s-3
,4-
.^
/£>
/-7
/ S)
£ -/
-^
3
-f-
3~
Position
Inches3
/,£>
/, .5-
-2. , £•
S~s &
£>, ,5"
o*^ /
>£?. 2-
/-^ 7
3S.3
^£<4-, ~%
&£,'?'
£tff,6
*£^7
5?^ *7
,^~^^G
33, JS"
Total
Average
Reading, Ap
"H2°
O<4*7
,5L5"
,^7
.foD
/
/S6
.57
y^O
• (al
_ittl
• S~l
'5~Ja
\ /
V
/\
/ ^
-
-
\/Ap
m O
S
F
&o
1
I
>V
a) From outside of port to sampling
Pi tot tube XS
Test No . ~7~s*isi*i*r^e.
Loc a t i on /&/&/ (js>&4z./'
Stack Inside Dimensions O/f^J -z> / s 7? '
S\<*. /sr A4>?y S^rss.
Stack Area, A = sq. ft.
s
Barometric Pressure , P. — .12. 7 *jo HQ
D ' 3
Stack Gage Pressure = — O»4L, "H-0
. .._ £
sudCK AJJS . rjressure, v — M9U + ", — M<
15.6 b
otacK oas lemp. / i^ — F T 460 — R
Molecular Weight of Stack Gas, M =
V— 1 "1 A \ /A i-> r"r\ \l T v OQ QO v OO* ^«-/m';^
j. / 4 v "P ^"P v * t; * /y.y^ x zy rt/min.
Ms
v= •=
Q, Volume = f t/min. x sq. ft. = cfn
Q , Standard Volume at 70°F and 29.92 "Hg (Wet Basis) =
Q x 530 x Ps = 17.7 x x
T 29.92
Qs - Qw x (ioo-w)/ioo =
point.
Manometer
Thermometer Otft-i-
Data Recorder 6j (^
Date & /!/<)/
,/f7U
. PEDCo- ENVIRONMENTAL
SUITE B • ATKINSON SQUARE
CINCINNATI. OHIO -452 './I 6
513 /771-433O
-------
NOMOGRAPH DATA
PLANT
DATE
A/0\/. "72.
SAMPLING LOCATION
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20 °F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
T(navg.
^0
pm
PS
PVP
'•m
savg.
APavg.
APmax.
''&*
0,~?5<£Srr>
<30
z
3.9. ^5
J9^at&t£>
-/.2
/O
-------
NOMOGRAPH DATA
PLANT
DATE
ST&A/
0 V, ~?Z
SAMPLING LOCATION
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
/fssv~je&
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),0F
/ySOf/7-*gV
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. tig
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in. '
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
Tmavg.
BWO
pm
ps
PVP
/rm
savg.
APavg.
^Prnax.
/^b
&,-?5e/h
76
Z
z?'3X
CjH«fl!^J£jgl_
-0.42
/.O
90
<3,&o
0.6?
<$.%2
*C ./^S-TgSTZ-
. ZSo-TevST-3 ^5^
// •*
/,7V
EPA(Dur)234
/
-------
NOMOGRAPH DATA
PLANT
DATE ~7 A/0 V. "7Z
SAMPLING LOCATION
. CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
/tS£i;*1tZl>
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),°F
P/ERCENT7|ifSfsTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 * STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
Tmavg.
Bwo
Pm
ps
PVP
/rm
savg.
Apavg.
^Pmax.
14*
//o
2
27.7P
-•2-7
1,0
-70
a-?o
/.~70
^^
- /P75"
, /?75
/•65
EPA (Our) 234
4/72
-------
APPENDIX E
SAMPLING PROCEDURES
-------
DETERMINATION OF PARTICULATE EMISSIONS FROM STATIONARY SOURCES
INTRODUCTION
The following method was used in this test program.
Sampling and analytical procedures followed those described
in the Federal Register.
SAMPLING APPARATUS
The particulate sampling train in the procedure used
in these tests met design specifications established by the
EPA.
Nozzle - Stainless steel (316) with sharp, tapered leading
edge.
Probe - Pyrex glass with a heating system capable of maintaining
a minimum gas temperature of 250°F at the exit end during
sampling and prevent condensation from occurring. No heating of
the probe was done in this test.
Pitot Tube - Type S attached to probe'to monitor stack gas
velocity.
Filter Holder - Pyrex glass with heating system capable of
maintaining minimum temperature of 225°F. No heating of the
probe was done in these tests.
1. Federal Register, Vol. 36, No. 247, Part II - Thursday,
Dec. 23, 1971.
E-l
-------
Impingers - Four impingers connected in series with glass
ball joints. The first, third, and fourth impingers were
of the Greenburg-Smith design, modified by replacing the
tip with a 1/2 inch I.D. glass tube extending to 1/2 inch
from the bottom of the flask. The second impinger was of
the Greenburg-Smith design with a standard tip.
Metering System - Vacuum gauge, leak-free pump, thermometers
capable of measuring temperature to within 5°F, dry gas
meter with 2% accuracy, and related equipment, or equivalent,
as needed to maintain an isokinetic sampling rate and to
determine sample volume.
Barometer - To measure atmospheric pressures to +^0.1 inches
Hg.. . •
SAMPLING PROCEDURE
After selecting the sampling site and the minimum
number of traverse points, the stack pressure, temperature,
moisture, and range of velocity head were measured according
to procedures described in Method 1 of the Federal Register
(December 23, 1971).
Approximately 200 grams of silica gel was weighed in
a sealed impinger prior to each test. Glass fiber filters*
(3" diameter) were desiccated for at least 24 hours and
* MSA 1106 BH
E-2
-------
weighed to the nearest 0.1 ing. One-hundred ml. of distilled
water was placed in each of the first two impingers; the third
impinger was initially empty; and the impinger containing the
silica gel was placed next in series. The train was set up
without the probe as shown in Figure A-l. The sampling
train was leak checked at the sampling site by plugging the
inlet to the filter holder and pulling a 15 in. Hg vacuum.
Leakage rates of less than 0.02 cfm at a vacuum of 15 in.
Hg were recorded in all cases. The probe assembly was then
attached and crushed ice was placed around the impingers.
More ice was added during the run to keep the temperature
of the gases leaving the last impinger at approximately
70°F.
During sampling, the data required on the meter data
sheet was recorded at each sampling point and when significant
changes in stack flow conditions required additional adjust-
ments in flow rate. Isokinetic sampling rates were set
throughout the sampling period with the aid of a nomograph
SAMPLE RECOVERY PROCEDURE
The sampling train was moved carefully from the test
site to the cleanup area at the plant. Samples of the
acetone and water used in the sample recovery were taken for
use as blanks. The sample fractions were recovered as
follows:
E-3
-------
o
\
\ ,
rtXh
(J-
1. - S. S. Nozzle
2. - S. S. Union
3. - Probe
4. - Cyclone (Optional)
5. - Glass Filter Holder
6. - Heated Box
7. - Ice Bath
8. - Modified G-S Imp.
9. - G-S Impinger
10. - Modified G-S Imp.
11. - Modified G-S Imp.
12. -• Thermometers
13. - Check Valve
14. - Umbilical Cord
15. - Vacuum Gauge
16. - Valve
17. - Leak-Free Pump
18. - By-Pass Valve
19. - Dry Gas Test Meter
20. - Orifice
21. - Dual Manometer
22. - S Pitot Tube
Figure A-l Particulate Sampling Train
E-4
-------
Container No. 1 - The filter was removed from its
holder and placed in a petri dish and sealed.
Container No. 2 - Loose particulate and acetone
washings from all sample-exposed surface prior to
the filter were placed in a glass jar and sealed.
Container No. 3 - The condensate from the first
three Greenburg-Smith impingers was measured with-
in + 1 ml. and placed into a glass jar. Water
rinsings from the back half of the filter holder,
the fritted glass support, all connectors, and
the first three Greenburg-Smith impingers were
placed in this container and the container sealed
with tape.
Container No. 4 - Acetone rinsings from the
back half of the filter holder, the fritted
glass support, all connectors, and the first
three Greenburg-Smith impingers were placed
in this container and.sealed.
The silica gel from the fourth impinger was weighed
and recorded. The used silica gel was discarded.
ANALYTICAL PROCEDURES
All data was recorded on the Analytical Data Sheets
included in Appendix F. The following procedures were
used and followed the methods described in the Federal
Register of August 17, 1971.
Container No. 1 - The filter and any loose
particulate matter from this sample container
was placed into tared glass weighing dish,
desiccated to a constant weight and weighed
to the nearest 0.1 mg.
1. Federal Register August 17, 1971, Vol. 36, No. 159
Part II, Pg. 15717.
E-5
-------
Container No. 2 - The acetone washings were
transferred to a tared beaker and evaporated
to dryness at ambient temperature and pressure;
desiccated to a constant weight; and weighed to
the nearest 0.1 mg.
Container No. 3 - Organic matter from the impinger
solution was extracted with three 25 ml. portions
each of ethyl ether and chloroform. The extracts
were combined into a tared beaker; evaporated
until no solvent remained at about 70°F. The
sample was then desiccated to.a constant weight
and weighed to the nearest O.i mg. The remaining
water was evaporated by boiling in a tared beaker,
and the residue weighed.
Container No. 4 - The acetone washings from the
back half of the filter holder, fritted support,
connectors and first three Greenburg-Smith
impingers were transferred to a tared beaker> and
evaporated to dryness at ambient temperature and
pressure. The sample was then desiccated to a
constant weight and weighed to the nearest 0.1 mg.
The total particulate weight was obtained by totaling
the weights of the individual sample components. The front
half of the sample consisted only of the filter and probe
washings. All liquid fractions were corrected for acetone
and distilled water blank values.
E-6
-------
APPENDIX F
LABORATORY REPORT
-------
CASCADE" I
CO.
P/V 3082-O
7.
i
Ui
' £
HMm&mLAUTLEL
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"
"
5. -...".
" QOTLgTl
ii
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PZLLBT CO.QU8jA!t6
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_5_60_
2.35
J=t3Q-
5Sf
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37£>-
-------
I'A-.CAOI ' I 1 . .'.•.(..•
I
IPELLeT COOtEf?
5 "
7
9
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235
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370
-------
PEDCo- ENVIRONMENTAL
SUITE 8 • ATKINSON SQUARE
CINCINNATI. OHIO 45246
PLANT.
DATE.
S •70*'
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
'
SAMPLE BOX NUMBER "
CLEAN-UP MAN 73. Ger*.SrL£
ANALYTICAL DATA
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS^.
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
2.OOO5
CONTAINER
55
CONTAINER 72-001- 95V
LABORATORY RESULTS
X 0 mg
O- /
.mg
FRONT HALF SUBTOTAL /95Q.1
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
7.5-
ETHER-CHLOROFORM
EXTRACTION 72-00,-
33-3- l.o
BACK HALF SUBTOTAL
.mg
32,3
2 -
mK
TOTAL WEIGHT
A793.8 m
MOISTURE
IMPINGERS
FINAL VOLUME
INITIAL'
SILICA GEL
FINAL WEIGHT
INITIAL
NET WEIGHT
ml
ml
.g
.g
• g
g
g
£
TOTAL MOISTURE
-------
PEDCo-ENVIRONMENTAL-
SUITE 8 • ATKINSON SQUARE
CINCINNATI. OHIO 4.524.6
ANALYTICAL DATA
PLANT
OATF
SAMPLING LOCATION
SAMPLFTYPF
RUN NUMBER
2a
SAMPLE BOX NUMBER
CLEAN-UP MAN
Loi/t&vut* COMMENTS:
J $ • $
ETHER-CHLOROFORffl
EXTRACTION v-a>/-ft
BACK HALF SUBTOTAL 37-1
mg
mg
mg
mg
TOTAI WFlfiHT ?#-G
mg
MOISTURE
IMPINGERS
FINAL VOLUME .
INITIAL VOLUME.
NET VOLUME .
| Q6 -
ml
ml
SILICA GEL (446.7
FINAL WEIGHT $60^ g
INITIAL WEIGHT <"T$-7 g
NET WEIGHT ^" 3 g
.g
.g
.g
TOTAL MOISTURE -
-------
PEDCo-ENVIRONMENTAL-
SUITE S • ATKINSON SQUARE
CINCINNATI. OHIO 4524.6
PLANT.
DATE_
ANALYTICAL DATA
SAMPLING LOCATION
SAMPLE TYPE _
RUN NUMBER _
SAMPLE BOX NUMBER.
CLEAN-UP MAN
7
COMMENTS:
/*sJ-£
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
Mfc FRONT HALF OF FILTER HOLDER
FILTER NUMBER 2-OOoSl£~
8//,7-z--z.
CONTAINERS
CONTAINER 7 L-
LABORATORY RESULTS
§_ mg
/2,5
-------
PEDCo - ENVIRONMENTAL
SUITE 8 • ATKINSON SQUARE
CINCINNATI. OHIO 45246
PLANT
DATE
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
SAMPLE BOX NUMBER.
CLEAN-UP MAN _
ANALYTICAL DATA
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
l
FILTER NUMBER •&
CONTAINER 72-OQI
CONTAINER 12-&>
LABORATORY RESULTS
73-0
.mg
FRONT HALF SUBTOTAL
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
MOISTURE
7.9 -o.fe
ETHER-CHLOROFORM
EXTRACTION^-"*5'-™*-0 4.5
CONTAINER 7Z-tx>i-
-------
PEDCo-ENVIRONMENTAL
SUITE 8 • ATKINSON SQUARE
CINCINNATI. OHIO 45246
PLANT.
DATE^
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
SAMPLE BOX NUMBER
CLEAN-UP MAN
7
ANALYTICAL DATA
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER 3Onf)6O
CONTAINER 7ZW-
CONTAINER 72- OOl-
LABORATORY RESULTS
"Z ggi. 9 mg
FRONT HALF SUBTOTAL 2££o. 7
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
t.7--»
ETHER-CHLOROFORM
EXTRACTION TZ-«W •*«-«>
CONTAINER 7^-^o/-
-------
ANALYTICAL DATA
PLANT
DATF
SAMPLING LOCATION
SAMPLE TYPE
RUNNHMRFR
SAMPLE BOX NUMBER
CLEAN-UP MAN
COMMENTS:
r
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS), CONTAINER
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER 2&&?5'S CONTAINER
LABORATORY RESULTS
.mg
FRONT HALF SUBTOTAL
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
CONTAINER
ETHER-CHLOROFORM
EXTRACTION 7^-
CONTAINER
BACK HALF SUBTOTAL
TOTAL WEIGHT
.mg
.mg
_mg
MOISTURE
IMPINGERS
FINAL VOLUME
INITIAL VOLUME
' NET VOLUME
ml
ml
ml
SILICA GEL ^£4-2*6
FINAL WEIGHT K—
INITIAL WEIGHT
NET WEIGHT
TOTAL MOISTURE
-------
PLANT
DATF
7 A/tfiS,
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER
SAMPLE BOX NUMBER
CLEAN-UP MAN
ANALYTICAL DATA
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
LABORATORY RESULTS
CONTAINER ZZ-a0/-
CONTAINER
.mg
FRONT HALF SUBTOTAL
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
ETHER-CHLOROFORM
EXTRACTION 7*
CONTAINER
BACK HALF SUBTOTAL
TOTAL WEIGHT
.mg
.mg
.mg
.mg
_mg
MOISTURE
IMPINGERS
FINAL VOLUME
INITIAL VOLUME
NET VOLUME
200
ml
ml
ml '
SILICA GEL W
FINAL WEIGHT 73?. 0 g
INITIAL WEIGHT ^^ ** g
NET WEIGHT 29'& g
TOTAL MOISTURE
-------
PEDCo-ENVIRONMENTAL
SUITE 8 • ATKINSON SQUARE
CINCINNATI. OHIO 4S246
ANALYTICAL DATA
PLANT
DATF 7 A/t?vx. "7Z
SAMPLING LOCATION
SAMPLE TYPE _
RUN NUMBER_
<"••>
SAMPLE BOX NUMBER
CLEAN-UP HAN
T
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
CONTAINER 7Z-4QI-'
LABORATORY RESULTS
.2 mg
BACK HALF
IMPINGER CONTENTS AND V/ATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
FRONT HALF SUBTOTAL
57/7
(o.l-O.*
r.nNTAINFR72-78,(o g
INITIAL WEIGHT 6&3-S g
NET WEIGHT
g
g
gi
TOTAL MOISTURE
-------
PEDCo- ENVIRONMENTAL
SUITE 8 . ATKINSON SQUARE
CINCINNATI. OHIO 4S2-46
PLANT.
DATE.
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
SAMPLE BOX NUMBER.
CLEAN-UP "~
ANALYTICAL DATA
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF FILTER HOLDER
FILTER NUMBER
CONTAINER
LABORATORY RESULTS
CONTAINER
FRONT HALF SUBTOTAL
.mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
7-S-0-0!
ETHER-CHLOROFORM
2.4
CONTAINER.
BACK HALF SUBTOTAL
.mg
.mg
.mg
.mg
TOTAL WEIGHT
£9-7
mg
MOISTURE
IMPINGERS
FINAL VOLUME _L££_ ml
INITIAL VOLUME _L££_ ml
NET VOLUME ml
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
. E
/ g
8
.g
.8
TOTAL MOISTURE
-------
APPENDIX G. TEST LOG
Personnel:
EPA:
PEDCo:
Tom Ward, Project Officer
Bill Mitchell
Roy Neulich't
Ken Woodard
R. Amick
R. Gerstle
E. Meer
G. Forte
Ralston Purina: J. Ballentine
DATE
TIME
11/6/72 800
800-1320
1320-1536
1625-1740
1920-2140
1920-2140
11/7/72 800
800-1230
1100-1330
1230-1330
1330-1430
1430-1500
EVENT
PEDCo crew arrives at Ralston Purina Feed
Plant in Louisville, Kentucky
Preparation for tests on pellet cooler
cyclone
Tests 1 and 2 on pellet cooler cyclone
Tests 3 and 4 on pellet cooler cyclone
Tests 5 and 6 on pellet cooler cyclone
13-15 minute break after one hour to
change product
Tests 5 and 6 on pellet cooler cyclone
PEDCo crew arrival at plant
Preparation for hammermill cyclone tests
(in,c61d rain)
R. Gerstle and G. Forte return to Cincinnati
First half of test 7 on hammermill
cyclone
Lunch
Finish Test 7
-------
DATE TIME EVENT
11/7/72 1620-1700 Test 8 on Hairanermill cyclone
1830-1940 Test 9 on Hammermi11 cyclone
1940-2100 Clean up trains
11/8/72 800-1100 Clean up test area, pack equipment,
load truck.
1100-1200 Lunch
1200-1400 Drive van to Cincinnati
-------
APPENDIX I. PROJECT PARTICIPANTS AND TITLES
Ralston Purina Co.
Louisville, Kentucky
EPA (GAP)
Tom Ward - Project Officer, ETB
Ken Woodard - Chemical Engineer, ESED
Bill Mitchell - QAMEL
Roy Neulicht - ETB
Ralston Purina
Jim Ballentine - Plant Manager
PEDCo
R. Gerstle, P.E. - Engineering Supervisor and
Field Supervisor
R. Amick - Environmental Engineer and Assistant
Field Supervisor
G. Forte - Technician
E. Meer - Technician
------- |