MIDWEST RESEARCH INSTITUTE
                                 MRI
EPORT
                SULFURIC ACID EMISSION TESTING OF A POWER PLANT

                                    at

                            Shawnee Power Station
                              Paducah, Kentucky

                       EPA Project Report No. 74-SPP9
                                    by
                             William H. Maxwell

                         Midwest Research Institute
                         EPA Contract No. 68-02-0228

                        MRI Project No. 3585-C,  Task 41

                                     For

                        Emission Measurements Branch
                  Office of Air Quality Planning  and Standards
                       Environmental Protection  Agency
                 Research Triangle Park, North Carolina  27711

                         Attn: Mr. Peter R.  Westlin
MIDWEST RESEARCH INSTITUTE 425 VOLKER BOULEVARD, KANSAS CITY, MISSOURI 64110  •  816561-0202

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                                  DISCLAIMER
             This  report was  furnished  to  the Environmental Protection
             Agency by Midwest  Research Institute,  Kansas City, Missouri,
             in  fulfillment of  Contract No.  68-02-0228,  Task No. 24.  The
             contents of this report  are reproduced herein as received
             from  the Midwest Research  Institute.   The opinions, findings,
             and conclusions  expressed  are those of the  author and not
             necessarily those  of the Environmental Protection Agency.
             Mention of company or product names is not  to be considered
             as  an endorsement  by the Environmental Protection Agency.
MRI WASHINGTON, D.C. 20005-1522 K STREET, N.W. • 202 293-3800

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                SULFURIC ACID EMISSION TESTING OF A POWER PLANT

                                       at

                              Shawnee Power Station
                                Paducah, Kentucky

                         EPA Project Report No. 74-SPP9
                                       by
                              William H. Maxwell
                           Midwest Research Institute
                           EPA Contract No. 68-02-0228

                        MRI Project No. 3585-C, Task 41
                                       For
                          Emission Measurements Branch
                   Office of Air Quality Planning and Standards
                         Environmental Protection Agency
                  Research Triangle Park, North Carolina  27711

                           Attn:  Mr.  Peter R.  Westlin
MIDWEST RESEARCH INSTITUTE 425 VOLKER BOULEVARD, KANSAS CITY, MISSOURI 64110 • 816561-0202

-------
                SULFURIC ACID EMISSION TESTING OF A POWER PLANT

                                       at

                              Shawnee Power Station
                                Paducah,  Kentucky

                         EPA Project Report No. 74-SPP9
                                       by
                              William H.  Maxwell
                           Midwest Research Institute
                           EPA Contract No. 68-02-0228

                        MRI Project No. 3585-C, Task 41
                                       For
                          Emission Measurements Branch
                   Office  of Air Quality Planning and Standards
                        Environmental Protection Agency
                  Research Triangle Park,  North Carolina  27711

                           Attn:  Mr.  Peter R.  Westlin
MIDWEST RESEARCH INSTITUTE 425 VOLKER BOULEVARD, KANSAS CITY, MISSOURI 64110 • 816561-0202

-------
                                   PREFACE
          The work reported herein was conducted by Midwest Research In-
stitute (MRI) under Environmental Protection Agency (EPA) Contract No.
68-02-0228, Task No. 37, Change No. 1.

          The project was under the technical supervision of Mr. Paul C.
Constant, Jr., Head, Environmental Measurements Section of the Physical
Sciences Division.  Mr. William Maxwell served as Crew Chief and was
assisted by Messrs. Emile Baladi, George Cobb, Bruce DaRos, and John Kitko.
Miss Christine Guenther was responsible for the data reduction and computer
analysis.  The analysis of the samples was done by Mr. Thurmon Oliver.
Approved for:

MIDWEST RESEARCH INSTITUTE
Paul C. Constant, Jr.,
Program Manager
21 May 1974
                                    ii

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                            TABLE OF CONTENTS
I.     Introduction	     1

II.    Summary of Results	     1

III.   Process Description	     3

IV.    Location of Sampling Ports	  .     4

V.     Sampling and Analytical Procedures	     4

VI.    Discussion	     5

Appendix A - Results of Analysis - Printout of Computer
               Calculations	     7

Appendix B - Sample Calculations 	    21

Appendix C - Field Data Sheets	    26
                                    iii

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                            I.  INTRODUCTION
          This report presents the results of source testing performed by
Midwest Research Institute on a pilot-plant scale wet scrubber at the
Shawnee Power Station, Paducah, Kentucky.  Three tests each for I^SO, mist
and S02 were run on the inlet and outlet ducts to the scrubber.

          The purpose of the testing was to determine the efficiency of a
wet scrubber in removing l^SO, .  The data were to be used in conjunction
with comparison tests of in-stack and EPA Method 5 particulate sampling
methods.

          The scope of work for this project specified:  three simultaneous
tests on the inlet and outlet of the scrubber to be completed in accordance
with the Federal Register, Vol, 36, No. 159, Part II, 17 August 1971.  Sam-
pling was completed with one test being run on 19 February 1974 and two tests
on 20 February 1974.

          The following sections of this report present:  (1) the summary
of results, (2) the process description, (3) the location of sampling ports,
(4) sampling and analytical procedures, and (5) a discussion.
                         II.  SUMMARY OF RESULTS
          Table I contains a summary of results for this testing.  A com-
plete listing of the data and computer printout of the calculations is
found in Appendix A.  Sample calculations are found in Appendix B.

          The 02 data used in the determination of the stack-gas molecular
weight were obtained from the plant process information by EPA.  The COo
and CO data are representative of values obtained at other coal-fired power
plants tested.  Orsat analyses were not run during this testing.

          The values listed on the computer printout for the amount of water
collected are assumed values computed from moisture concentrations of 7% and
20% by volumes for the inlet and outlet ducts, respectively.

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N>
Concentration of HjSO,  - Ib/dscf
                       - mg/ncm
                       -.ppni
                       - Ib/hr
                       - kg/hr
                    .   - g/dscf
                       - g/acf
Percent efficiency
  of removal—'
      Concentration  of  SOj
        (total)
      Percent  efficiency
        of  removal—
                                                                           TABLE  I

                                                                     SUMMARY OF RESULTS
Run Number
1-Inlet
0.00000082
13.1
3.2
0.7
0.3
0.0057
0.0037
1 -Out let
0.00000043 .
7.0
1.7
0.3
0.2
0.0030
0.0024
2-Inlet
0.00000352
56.4
13.9
3.2
1-5
0.0247
0.0168
2-Outlet
0.00003170
507.7
125.1
26.6
12.1
0.2219
0.1764
3-Inlet
0.00017006
2,724.1
671.0
150.8
68.4
1.1904
0.8017
3-Outlet
0.0000082?
132.1
32.5
7.5
3.4
0.0577
0.0457
                                                        46.875
- Ib/dscf
- mg/ncm .
- ppm
- Ib/hr
- kg/hr
- g/dscf.
- g/acf
0.00019421
3,110.8
1,173.3
167.8
76.1
1.3594
0.8801
0.00005993
959.9
362.0
48.1
21.8
0.4194
0.3287
0.00037
51.8
2,244.7
339.1
153.8
2.6010
1.7675
                                                                                                   0.00011591
                                                                                                   1,856.6
                                                                                                   700.2
                                                                                                   97.1
                                                                                                   44.1
                                                                                                   0.8114
                                                                                                   0.6451
                                                                                                                                     95.156
0.00030421
4,872.9
1,837.9
269.8
122.4
2.1295
1.4341
0.00004210
674.4
254.3
38.4
17.4
0.2948
0.2332
                                                   69.146
                                                                                                68.807
        86.164
      aj    Obtained  from ppm values

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                         III.  PROCESS DESCRIPTION
           The Shawnee Power Station, operated by The Tennessee Valley
 Authority (TVA), is a coal-fired, steam-generation station, having  10
 turbines, each served by a boiler and stack.  A portion of  the exhaust
 gases from one of these stacks is diverted for use with three pilot-plant
 scale wet scrubber systems.  It was on one of these wet scrubber  systems
 that the current testing was done.  Figure 1 presents a flow diagram of
 the operation, showing the inlet and outlet sampling sites.
    Outlet
    Sampling
    Site ——
     Reheater
     Scrubber
                   Stack
 Main
 Stack
                   Fan
Inlet
Sampling
Site
                                                Boiler
                                                Turbine
                Figure 1 - Flow Diagram of Plant Operation
           The  scrubber  tested was a Bechtel Turbulent contact absorber de-
 signed  to  handle approximately 30,000 cfm of  exhaust gas.  Water was the
 scrubbing  medium flowing  concurrently over plastic spheres in the scrubber
.main  chamber.   Downstream of the scrubber were a demister and a reheater.

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                     IV.  LOCATION OF SAMPLING PORTS
          Both sampling locations were sited in enclosed sheds as protec-
tion against the weather.  Existing 4 in. ID ports were utilized.  Due to
the proximity of the shed wall to one of the outlet ports, complete traversing
on that port could not be accomplished.  It was decided on-site by EPA and
MRI personnel to run two traverses in the accessible port instead of only
partially traversing in the blocked port.  It was indicated that the sites
had been selected to comply with EPA guidelines so the minimum number of
points, 12, was used for the 2-hr tests.  Figure 2 shows a schematic layout
of the sampling sites and ports used.
             West
                 Outlet Site
                   Insufficient
                                  North
                                                •Shed Wall-
                  Figure 2 - Schematic of Sampling Sites
                  V.  SAMPLING AND ANALYTICAL PROCEDURES
          The samples were taken with Research Appliance Company (RAG)
Model 2243 "StacksampIr" equipment, as modified by MRI.  Sampling train ,
specifications were in accordance with the Federal Register. "Method 8 -
Determination of Sulfuric Acid Mist and Sulfur Dioxide Emissions from
Stationary Sources," Vol. 36, No. 159, 17 August 1971, with the following
exceptions:

          1.  An additional Greenburg-Smith impinger containing 100 ml of
80% isopropanol was placed in front of the filter between the isopropanol
and hydrogen peroxide.  This gave a total of five impingers:  two isopropanol,
two hydrogen peroxide,  and one silica gel.

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          2.  Due to the ash content of the inlet duct, a cyclone and a
filter were placed in front of the first isopropanol impinger.  After the
first run, this was also done for the outlet duct.

          3.  The system was purged for 30 min following each test.  These
exceptions were done upon the suggestion and approval of EPA.

          Sample recovery was done in the field in accordance with the
Federal Register except that the filters were not added to the isopropanol
wash of the probe and cyclone or the contents of the first two impingers
until they were returned to the lab at MRI.

          The analytical procedures were those described in the Federal
Register.  Due to the presence of the fly-ash material, in addition to the
filter material in the isopropanol solution, this solution was filtered
prior to analysis to observe the end point more easily.
                             VI.  DISCUSSION
          Sampling was done simultaneously on both sites over a 2-hr period.
There were two, six-point traverses per run, with each point sampled for
10 min.  Data were recorded every 5 min.  During the first run, it was discovered
that a 4-min timer was being used on the outlet duct, resulting in 8-min
points on the first traverse.  As the second traverse consisted merely of a
retracing of the first in the same port, the same tinier was used but for
12-min points on the second traverse to get the 2-hr total sample time.

          Large meter vacuum readings were encountered during the sampling
periods on both ducts.  This resulted partially from the high stack vacuum,
reported as being 14 in. of water, the increased number of impingers and
filters over that normally used for particulate sampling,and the high stack
grain loading which tended to plug the first filters.  At the higher vacuum
readings, the silica gel, on occasion, tended to boil, i.e., be physically
lifted by the gas flow in the impinger.  Due to the higher vacuums, it be-
came necessary to replace the first filter on the inlet train in order to
maintain isokinetic sampling conditions.  This was done once for runs 1
and 2 and twice on run 3.

          Complete traversing could be effected on the inlet duct but the
train could not be removed from the stack without first disconnecting the
probe.   Due to the high stack vacuum, this resulted in the loss of any
sample contained in the probe.  However, due to the large amount of mass
collected by the cyclone and filter, the loss is believed to be negligible.

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          During run 3, on the inlet duct, it was observed that the hydrogen
peroxide from the last impinger of the train was spilling over into the silica
gel impinger due to the large amount of froth resulting from the bubbling
action of the gas on the liquid.  This did not cease even when the first
filter was replaced.  No determination could be made as to how much was lost
but the resulting SC>2 data could be biased.

          When the samples were opened at MRI, it was noticed that all of the
hydrogen peroxide samples smelled of isopropanol indicating the perhaps some
of the isopropanol was carried over through the filter to the hydrogen per-
oxide.  This was not physically observed in the field.

          At least one reference (Industrial Source Sampling, Brenchley,
Turley, and Yarmac) states that Method 8 sampling should not be used on any
source having a high particulate load which could cause interferences with
the wet chemical analysis.  It is not known how this particulate load would
affect the sampling under study or if filtering the sample will remove the
interferences.

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                      APPENDIX A
RESULTS OF ANALYSIS - PRINTOUT OF COMPUTER CALCULATIONS

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                                      DATA,AND CALCULATED VALUES
                               RUN-
    1-1   DATE- 02-19-74
      ATMOS  ATMOS  STACK
      TEMP   PRES    VAC   COND
     (06.F) (I.HG) (I.H20) (ML)

      45.0   29.15  14.00  102.1
                 STACK  INIT   PERC PERC PERC PITOT
WT-PTL   KT-TTL   AREA   VOL    02   C02  CO   TUBE
 (M6)     (H6)   (FT2)  (DCF)    DRY  DRY  DRY  COEF

                  8.73  758.74  3.5 11.0  0.0  .850
00
PORT-
POINT

S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S

1
1
2
2
3
3
4
4
5
5
6
6
6
6
5
5
4
4'
3
3
.2
2
i
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
761.36
763.93
766.67
769.47
772.26
775.02
777.84
780.64
783.47
786.33
789.29
792.29
795.05
797.95
800.82
803.67
806.52
809.33
812.02
814.71
817.55
820.38
823.12
825.80
DELTA
P
I.H20)
.350
.360
.440
.450
.410
.410
.420
.420
.460
.450
.480
.470
.490
.490
.450
.450
.410
.410
.340
.325
.440
.440
.360
.360
DELTA
H
(I.H20)
.910
.930
1.140
1.160
1.080
1.080
1.090
1.090
1.180
1.150
1.230
1.210
1.260
1.260
1.160
1.160
1.080
1.080
.890
.840
1.140
1.140"
.930
.930
TEMP
IN
(D.F)
60.0
70.0
81.0
86.0
90.0
92.0
94.0
95.0
96.0
97.0
98.0
99.0
65.0
78.0
87.0
91.0
94.0
95.0
96.0
95.0
97.0
96.0
98.0
98.0
TEMP
OUT
(D.F)
47.0
46.0
51.0
53.0
57.0
59.0
62.0
63.0
64.0
66.0
67.0
68.0
61.0
61.0
62.0
63.0
64.0
65.0
66.0
67.0
68.0
68.0
69.0
70.0
TRAIN
VAC
(I.HG)
8.0
8.0
8.0
9.0
9.0
9.5
9.5
9.5
10.0
10.0
11.0
11.0
8.0
9.5
9.5
9.5
8.5
8.5
8.0
9.0
9.0
9.0
8.5
8.0
STACK
TEMP
(D.F)
310.0
309.0
320.0
316.0
315.0
314.0
316.0
315.0
312.0
314.0
315.0
315.0
314.0
311.0
310.0
312.0
309.0
305.0
301.0
300.0
300.0
299.0
29S.O
295.0
                                                                   BOX  PROBE
                                                                   TEMP T 01A   VEL
                                                                  (D.F) (IN)   (FPM)
                                                                   60.0
                                                                   65.0
                                                                   75.0
                                                                   65.0
                                                                   75.0
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
                                      .250
2502.2
2536.1
2823.7
2848.3
2717.0
2715.3
2751.7
2750.0
2872.4
2844.6
2939.8
2909.0
2968.4
2962.6
2837.3
2841.0
2706.5
2699.4
2451.8
2395.5
2787.3
2785.5
2512.9
2512.9

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            AND CALCOEATED~VA'LUE5~
RUN-
1-0   DATE- 02-19-74
ATHOS
TEMP
DQ.F)
45.0
PORT-
POINT

E
e
E
E
E
E
E
E
E
E
.E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
E
.E
E
E
E

1
1
2
2
3
3
4
4
5
5
6
6
6
6
6
5
5
5
4
4
4
3
3
3
2
2
2
1
1
1
ATMOS
PRES
(I.H6)
29.15
SAMP
TIME
(MIN)
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4.00
4*00
4,00
4.00
4.00
4.00
4.00
STACK
VAC
(I.H20)
14.00
METER
VOL
(OCF) (
299.69
301.69
303.78
305.61
307.93
310.17
312.36
314.57
316.77
318.96
321.01
322.96
324.89
326.59
328.43
330.20
331.92
333.66
335.40
337.15
338.85
340.90
343.00
345.07
347.11
349.13
351.10
352.95
354.72
356*47
H20
CONO
(ML)
300.5
DELTA
P
I.H20)
.420
.420
.450
.450
.470
.470
.480
.480
.440
.440
.360
.360
.360
.250
.250
.300
.300
.300
.300
.300
.300
.450
.450
.450
.440
.440
.440
.350
.350
.350
STACK INIT PERC PERC PERC PI TOT
WT-PTL WT-TTL AREA VOL 02 C02 CO TUBE
(MG) (M6) (FT2) (DCF) DRY DRY DRY COEF
8.73 297.54 3.5 11.0 0.0 .850
DELTA TEMP TEMP TRAIN STACK BOX PROBE
H
(I.H20)
.850
.850
.940
.940
.950
.950
.960
.960
.880
.880
.730
.730
.730
.530
.530
.610
.610
.610
.610
.610
.610
.930
.930
.930
.890
.890
.890
.710
.710
.710
IN
(D.F)
45.0
60.0
76.0
80.0
84.0
87.0
90.0
92.0
94.0
94.0
94.0
94.0
94.0
93.0
91.0
90.0
90.0
89.0
88.0
88.0
87.0
87.0
89.0
91.0
92.0
93.0
93.0
94.0
95.0
95.0
OUT
(D.F)
45.0
50.0
54.0
57.0
59.0
60.0
61.0
62.0
64.0
64.0
65.0
65.0
65.0
62.0
60.0
58.0
58.0
59.0
59.0
62.0
61.0
62.0
64.0
66.0
67.0
68.0
69.0
70.0
70.0
71.0
VAC
(I.HG)
11.0
11.0
11.0
12.0
13.0
13.0
13.0
13.0
13.0
12.5
12.0
12.0
12.0
12.0
12.0
11.0
11.0
11.0
11.0
11.0
11.0
17.0
20.0
21.0
23.0
23.0
23.0
23.0
23.0
23.0
TEMP TEMP
(D.F) (D.F)
150.0 50.0
150.0
160.0
160.0
170.0
170.0
170.0
170.0
170.0
170.0
200.0
200.0
200.0
200.0
200.0
180.0 75.0
180.0
180.0
180.0
180.0
180.0
175.0 80.0
175.0
175.0
180.0 80.0
180.0
180.0
160.0 75.0
160.0
160.0
T DIA
(IN)
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
,250
.250
.250
.250
.250
.250
.250
VEL
(FPM)
2507.6
2507.6
2616.8
2616.8
2695.8
2695.8
2724.3
2724.3
2608.3
2608.3
2414.8
2414.8
2414.3
2012.4
2012.4
2170.8
2170.8
2170.8
2170.8
2170.8
2170.8
2648.2
2648.2
2648.2
2628.9
2628.9
2628.9
2307.8
2307.8
2307.8

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                                 DATA AND CALCULATED VALUES
                          RUN-
                           2-1    DATE- 02-20-74
 ATMOS
 TEMP
(D0.F)

 40.0
 ATMOS
 PRES
(I.HG)
 STACK    H20
  VAC   COND
(I.H20)  (ML)
 29.84  14.00   102.7
WT-PTL
 (M6)
WT-TTL
 (M6)
STACK
 AREA
(FT2)
INIT
 VOL
(DCF)
                               PERC PERC PERC PITOT
02
DRY
C02
DRY
CO
DRY
TUBE
COEF
                                  8.73   839.55  3.5 11.0   0.0  .850
PORT-
POINT

S
S
S
S
S
S
S
S
S
s
S
S
S
S
S
S
S
S
S
S
S
S
S
S

1
1
2
2
3
3
4
4
5
5
6
6
6
6
5
5
4
4-
3
3
2
2
I
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
842.32
844.94
847.73
850.51
853.26
856.02
858.81
861.57
864.46
867.27
869.99
872.57
875.49
878.47
881.40
884.35
887.18
890.03
892.83
895.54
898.37
901.12-
903.78
906.44
DELTA
P
I.H20)
.370
.370
.450
.450
.410
.420
.430
.430
.480
.460
.500
.510
.500
.500
.490
.490
.430
.440
• 430
.440
.460
.460
.390
.390
DELTA
H
(I.H20)
.950
.950
1.180
1.180
1.080
1.100
1.130
1.130
1.230
1.230
1.000
.970
1.300
1.300
1.280
1.280
1.130
1.140
1.130
1.140
1.190
1,190
1.000
1.000
TEMP
IN
(D.F)
72.0
77.0
88.0
94.0
97.0
99.0
100.0
101.0
102.0
103.0
102.0
102.0
93.0
102.0
108.0
109.0
110.0
110.0
110.0
110.0
109.0
108.0
108.0
108.0
TEMP
OUT
(D.F)
56.0
64.0
66.0
67.0
68.0
70.0
71.0
72.0
74.0
74.0
76.0
76.0
76.0
76.0
78.0
79.0
79.0
80.0
81.0
81.0
82.0
82.0
83.0
83.0
TRAIN
VAC
(I.HG)
10.0
10.0
7.0
8.0
8.5
9.5
11.5
13.0
17.0
19.0
23.0
24.0
7.5
7.5
8.5
9.5
10.5
12.0
14.0
16.0
18.0
20.0
21.0
23.0
STACK
TEMP
(D.F)
290.0
284.0
290.0
29 1 . 0
291.0
294.0
291.0
293.0
293.0
293.0
290.0
291.0
293.0
295.0
300.0
291.0
291.0
294.0
290.0
290.0
290.0
291.0
279.0
285.0
                                                              BOX  PROBE
                                                              TEMP T 01A   VEL
                                                             (D.F) (IN)    (FPM)
                                                              50.0
                                                              50.0
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             ,250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                             .250
                                                           2508.8
                                                           2498.7
                                                           2766.7
                                                           2768.6
                                                           2642.7
                                                           2680.0
                                                           2706.3
                                                           2709.9
                                                           2863.2
                                                           2863.2
                                                           2916.4
                                                           2947.4
                                                           2922.2
                                                           2926.1
                                                           2906.3
                                                           2889.0
                                                           2706.3
                                                           2743.1
                                                           2704.5
                                                           2735.8
                                                           2797.3
                                                           2799.2
                                                           2556.7
                                                           2567.1

-------
                                 DATA AND CALCULATED VALUES
                          RUN-
                          2-0   DATE- 02-20-74
 ATMOS  ATMOS  STACK
 TEMP   PRES    VAC   COND    WT-PTL   WT-TTL
(D6.F) (I.HG)  (I.H20)  (ML)     (MO)      (M6)
 40.0
29.84  14.00  316.0
STACK  INIT   PERC PERC PERC PITOT
 AREA   VOL    02   C02  CO   TUBE

-------
                                 DATA AND CALCULATED  VALUES
                          RUN-
    3-1   DATE- Oa-20-74
 ATMOS  ATMOS  STACK    H20
 TEMP   PRES    VAC   COND
(OG»F) (I.HG) (I.H20)  (ML)

 50.0   29.90  14.00   101.3
                 STACK  IMT   PERC PERC PERC PITOT
WT-PTL   WT-TTL   AREA   VOL    02   C02  CO   TUBE
 
-------
                                       DATA AND CALCULATED VALUES
                                RUN-
                                  3-0   DATE- 03-20-74
 ATMOS  ATMOS  STACK   H20
 TEMP   PRES    VAC   COND
(DG.F) (I.HG) (I.H20)  (ML)

 50.0   29.90  14.00  341.2
                                                     STACK  INIT   PERC PERC PERC PITOT
                                    HT-PTL   KT-TTL   AREA   VOL    02   C02  CO   TUBE
                                     (M0)     (MG)   (FT2)  (DCF)   DRY  DRY  DRY  COEF

                                                      8.73  443.44  3.5 11.0  0.0  .850
u>
PORT-
POINT

E
E
E
E
E
E
••«.
E
E
-m
•E.
E
E
E
••'ft
E
E
E
-E
E
E
E
EV
E

1
1
2
2
3
3
4
4
5
5
6
6
6
6
5
5
4
. 4-
3
3
2
2
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (I
446.34
448.91
451.58
454.25
456.09
459.57
462.46
465.55
468.42
471.30
473.97
476.60
479.09
481.59
484.30
487.14
490.05
493,97
495.79
498.74
501.64
504.46
50*. 18
509.82
DELTA
P
• H20)
.470
.470
.520
.520
.470
.470
.500
.500
.520
.520
.450
.450
.400
.400
.510
.510
.570
.570
.510
.510
.520
.520
.450
.450
DELTA
H
(I.H20)
.930
.930
1.020
1.020
.930
.930
1*020
1.020
1.050
1.050
.910
.910
.810
.810
1.010
1.010
1.140
1.140
1.010
1.010
1.050
1.050
.910
.910
TEMP
IN
(D.F)
64.0
72.0
80.0
85.0
90.0
87.0
84.0
91.0
99.0
96.0
92.0
93.0
100.0
102.0
104.0
106.0
108.0
108.0
108.0
106.0
105.0
108.0
110.0
111.0
TEMP
OUT
(D.F*
62.0
62.0
63.0
64.0
65.0
66.0
68.0
69.0
70.0
71.0
72.0
73.0
74.0
75.0
77.0
78.0
79.0
79,0
78.0
79.0
80.0
81.0
82.0
83.0
TRAIN
VAC
(I.HG)
10.0
10.0
10.0
10.0
10.0
11.0
12.0
12.5
13.0
13.0
13.0
13.0
12.0
13.0
14.0
14.5
15.0
15.0
15.0
15.5
16.0
16.0
16*0
16.0
STACK
TEMP
(D.F)
195.0
195.0
195.0
195.0
195.0
195.0
195.0
195.0
180.0
180.0
180.0
180.0
180.0
180.0
185.0
185.0
185.0
185.0
185.0
185.0
180.0
180.0
180.0
180.0
BOX
TEMP
(D.F)
60.0

75.0

75.0

75.0

75.0

75.0

75.0

75.0

75.0

80.0

80.0

80.0

PROBE
T DIA
(IN)
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250
.250

VEL
(FPM)
2712.6
2712.8
2853.5
2853.5
2712.8
2712.8
2798.1
2798.1
2820.6
2820.6
2623.9
2623.9
2473.8
2473.8
2804.2
2804.2
2964.6
2964.6
2804.2
2804.2
2820.6
2820.6
2623.9
2623.9

-------
                       EMISSION DATA
NAME      DESCRIPTION            UNITS

       DATE OF RUN

ON     PROBE TIP DIAMETER           IN
tt     NET TIME OF RUN             MIN
PB     BAROMETRIC PRESSURE       IN.HG
PM     AV6 ORIFICE PRES DROP    IN.H20
VM     VOL DRY GAS-METER COND      DCF
TM     AVG GAS METER TEMP        DEG.F
VMSTD  VOL DRY 6AS-STD COND       DSCF
V*     TOTAL H20 COLLECTED          ML
VWV    VOL H20 VAPOR-STD COND      SCF
PMOS   PERCENT MOISTURE BY VOL
MO     MOLE FRACTION DRY GAS
RC02   PERCENT CQ2 BY VOLt DRY
IP02    PERCENT 02 BY VOL. DRY
PCO    PERCENT CO BY VOL » DRY
PN2    PERCENT N2 BY VOL» DRY
HMD    MOLECULAR WT-DRY STK GAS
Mt(     MOLECULAR HT-STK GAS
CP     PITOT TUBE COEFFICIENT
DPS    AVG STK VELOCITY HEAD    IN.H20
TS     AVG STACK TEMPERATURE     DEG.F
NP     NET SAMPLING POINTS
PST    STATIC PRES OF STACK      IN.HG
PS     STACK PRESSURE, ABSOLUTE  IN.HG
VS     AVG STACK GAS VELOCITY      FPM
AS     STACK AREA                  IN2
QS     SfK FLOWRATEt DRY»STD CN  DSCFM
OA     ACTUAL STACK FLOWRATE      ACFM
PfRl  _FfRCENT ISDKINET1C
EA"     PERCENT EXCESS'AIR                !
1-1
02-19-74
.250
120.0
29.15
1.088
67.06
75.8
64.80
102.1
4.84
6.949
.931
11.0
3.5
0.0
85.5
29.90
29.07
.850
.420
309.3
24
-1.03
28.12
2737
1257
14398
23895
95.8
18. "4
1-0
02-19-74
.250
120.0
29.15
.789
58.93
74.8
57.01
300.5
14.24
19.989
.800
11.0
3.5
0.0
85.5
29.90
27.52
.850
.387
175.5
30
-1.03
28.12
2446
1257
13391
21352
90.6
18.4
2-1
02-20-74
.250
120.0
29.84
1.134
66.89
87.8
64.72
102.7
4.87
6.995
.930
11.0
3.5
0.0
85.5
29.90
29.07
.850
.447
290.8
24
-1.03
28.81
2756
1257
15210
24060
90.5
18.4
2-0
02-20-74
.250
120.0
29.84
.834
61.43
82.9
59.93
316.0
14.98
19.995
.600
11.0
3.5
0.0
85.5
29.90
27.52
.850
.413
181.7
24
-1.03
26.81
2515
1257
13971
21955
91.3
18.4

-------
                EMISSION DATA
NAME
DN
TT
PB
PM
VN
TM
VMSTD
V»
VWV
PMOS
MD
PC02
P02
PCO
PN2
MttD
K%
CP
DPS
TS
MP
PST
PS
VS
AS
QS
QA
   DESCRIPTION            UNITS

DATE OF RUN

PROBE TIP DIAMETER           IN
NET TIME OF RUN             MIN
BAROMETRIC PRESSURE       IN.HG
AVG ORIFICE PRES DROP    IN.H20
VOL DRY GAS-METER COND      DCF
AVG GAS METER TEMP        DEG.F
VOL DRY GAS-STD COND       DSCF
TOTAL H20 COLLECTED          ML
VOL H20 VAPOR-STO COND      SCF
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL* DRY
PERCENT 02 BY VOL. DRV
PERCENT CO BY VOL» DRY
PERCENT N2 BY VOL» DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY MEAD    IN.H20
AV0 STACK TEMPERATURE     DEG.F
NET SAMPLING POINTS
STATIC PRES OF STACK      IN.HG
STACK PRESSURE, ABSOLUTE  IN.HG
AVG STACK GAS VELOCITY      FPM
STACK AREA                  IN2
STK FLOWRATE* DRY.STD CN  DSCFM
ACTUAL STACK FLOWRATE      ACFM
        J50KINETJLC:  ,
EA
PERCENT EXCESS AIR
3*1
02-20-74
.250
120.0
29.90
1.096
66.77
95.9
63.79
101.3
4.80
7.000
.930
11.0
3.5
0.0
85.5
29.90
29.07
.850
.426
299.2
24
-1.03
28.87
2704
1257
14789
23606
91.8
18.4
3-0
02-20-74
.250
120.0
29.90
.982
66.38
84.6
64.72
341.2
16.17
19.994
.800
11.0
3.5
0.0
85.5
29.90
27.52
.650
.491
186.3
24
-1.03
28.87
2752
1257
15211
24024
90.5
18.4

-------
                              EMISSION DATA
                             (METRIC RESULTS)
NAME      DESCRIPTION

       DATE OF RUN

ON     PROBE TIP DIAMETER
TT     NET TIME OF RUN
PB     BAROMETRIC PRESSURE
PM     AVG ORIFICE PRES DROP
VM     VOL DRY GAS-METER COND
TM     AVG GAS METER TEMP
VMSTM  VOL DRY GAS-STD COND
V«     TOTAL H2O COLLECTED
VWM    VOL H20 VAPOR-STD COND
PMOS   PERCENT MOISTURE BY VOL
MD     MOLE FRACTION DRY GAS
PC02   PERCENT C02 BY VOL» DRY
P02    PERCENT 02 BY VOL* DRY
PCO    PERCENT CO BY VOL* DRY
PNE    PERCENT NZ BY VOL* DRY
HMD    MOLECULAR WT-DRY STK GAS
MM     MOLECULAR WT-STK GAS
CP     PITOT TUBE COEFFICIENT
DPS    AVG STK VELOCITY HEAD
TSM    AVG STACK TEMPERATURE
NP     NET SAMPLING POINTS
PST    STATIC PRES OF STACK
PS     STACK PRESSURE* ABSOLUTE
VSM    AVG STACK GAS VELOCITY
AS     STACK AREA
QSM    STK FLOWRATE* DRY»STD CN
0AM    ACTUAL STACK FLOURATE
PERI   PERCENT ISDKINET1C
UNITS

IN
MIN
IN.HG
IN.H20
DCF
DEG.F
NCM
ML
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
M3/MIN

1-1
02-19-7*
.250
120.0
29.15
1 . 088
67.06
75.8
1.84
102.1
.14
6.949
.931
11.0
3.5
0.0
85.5
29.90
29.07
.850
.420
154.0
24
-1.03
28.12
834.4
1257
407.71
676.64
95*8
1-0
02-19-74
.250
120.0
29.15
.789
58.93
74.8
1.61
300.5
.40
19.989
.800
11.0
3.5
0.0
85.5
29.90
27.52
.850
.387
79.7
30
-1.03
28.12
745.6
1257
379.20
604.64
90.6
2-1
02-20-74
.250
120.0
29.84
1.134
66.89
87.8
1.83
102.7
.14
6.995
.930
11.0
3.5
0.0
85.5
29.90
29.07
.850
.447
143.8
24
-1.03
28.81
840.1
1257
430.70
681.32
90.5
2-0
02-20-74
.250
120.0
29.84
.834
61.43
82.9
1.70
316.0
.42
19.995
.800
11.0
3.5
0.0
85.5
29.90
27.52
.850
.413
83.1
24
-1.03
28.81
766.6
1257
395.61
621.71
91.3

-------
                              EMISSION DATA
                             (METRIC RESULTS)
NAME      DESCRIPTION

       DATE OF RUN

ON     PROBE TIP DIAMETER
TT     NET TIME OF RUN
PB     BAROMETRIC PRESSURE
PM     AVG ORIFICE PRES DROP
VM     VOL DRY GAS-METER COND
TM     AVG GAS METER TEMP
VMSTM  VOL DRY GAS-STD COND
y«     TOTAL H20 COLLECTED
VMM    VOL H20 VAPOR-STD COND
PMOS   PERCENT MOISTURE BY VOL
MD     MOLE FRACTION DRY GAS
PC02   PERCENT C02 BY VOL* DRY
P02    PERCENT 02 BY VOL. DRY
PCO    PERCENT CO BY VOL. DRY
PH8    PERCENT N2 BY VOLt DRY
MWD    MOLECULAR MT-DRY STK GAS
Mil     MOLECULAR WT-STK GAS
CP     PITOT TUBE COEFFICIENT
DPS    AVG STK VELOCITY HEAD
TSM    AVG STACK TEMPERATURE
NP     NET SAMPLING POINTS
PST    STATIC PRES OF STACK
PS     STACK PRESSURE. ABSOLUTE
VSM    AVG STACK GAS VELOCITY
AS     STACK AREA
OSM    STK FLOWRATE. DRYfSTD CN
QAM    ACTUAL STACK FLOWRATE
PERI   PERCENT .ISOKINETIC
UNITS

IN
MIN
IN.HG
IN.H20
DCF
DEG.F
NCM
ML
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
M3/MIN

3-1
02-20-74
.250
120.0
29.90
1.096
66.77
95.9
1.81
101.3
.14
7.000
.930
11. 0
3.5
0.0
85.5
29.90
29.07
.650
.426
148.4
24
-1.03
28.87
824,3
1257
418.78
668.46
91.8
3-0
02^20-74
.250
120.0
29.90
.982
66.38
84.6
1.83
341.2
.46
19.994
.800
11.0
3.5
0.0
85.5
29.90
27.52
.850
.491
85.7
24
-1.03
28.87
838.9
1257
430.72
680.30
90.5

-------
                                             AMAI YSTS  DATA
oo
NAME


VM
TM
PM
VMSTD
QT
VT
VTB
N
VSOLN
VA
CS02


DESCRIPTION
DATE
PORT
POINT
SAMPLE
VOL OF DRY GAS-METER CN
AVG DRY GAS METER TEMP
AVfi ARS METER PRES
VOL OF DRY GAS-STD CN
STK FLOWRATEt DRYtSTD CN
VOL OF TITRANT-SAMPLE
VOL OF TITRANT-ABS BLANK
NORMAI ITY OF TTTRANT
TOTAL SOLUTION VOLUME
VOL SAMP ALIQUOT TITRD
CQNC OF SAMPLE-STD CN L


UNITS


CU.FT
DEG.R
IN.Hfi
CU.FT
DSCFM
ML
ML
G-FQ/L
ML
ML
fl/DSCF
PPM
L8/HR
GR/DSCF
GR/ACF
MG/NM3
KG/HR
1-1
02-19-74
S02 -
67.06
535.80
Zfl.12
64.80
14398.0
283.00
.10
.10050
230.0
40.0
1074.5
153.7
L.Z450
.8060
2849.0
69.69

02-19-74
s
1 S02 -2
67.06
535.80
64.80
14398.0
26.10
.10
_ -.11)050.
230.0
40.0
^o.aaoi635_
98.8
14.1
.1144
.0741
261.8
. . 16...A.1 -
1-T
02-19-74
s
H2S04'
67.06
535.80
64.80
14398.0
.40
.10
.10050
650.0
40.0
,00000082
1-0
02-19-74
W
S02 -1
58.93
534.80
57.01
13391.0
66.00
.10
T10050
290.0
40.0
.0000591ft ,
3.2 358.7
.7 47.7
.0057 .415ft
.0037
13.1
.3257
951.1
l-o
02-19-74
w
S02 -2
58.93
534.80
57.01
13391.0
1.63
.10
115.0
40.0
• 0 Q-Q 0 Ou.33 — «
3.3
.4
.0038
.0030
8.8
	 - .20.-:
1-0
02-19-74
W
H2S04
58.93
534.80
57.01
13391.0
.35
.10
.10050
365.0
40.0
* 1.7
.3
.0030
.0024
7.0
_ - -._. .16

-------
ANALYSTS DATA
NAME


\l»
TM
PM
VMSTD
QT
VT
VTB
N
VSOLN
VA
CS02


DESCRIPTION
DATE
PORT
POINT
SAMPLE
VOL OF DHY GAS-METER CN
AVG DRY GAS METER TEMP
AVG ABS METER PRES
VOL OF DRY GAS-STD CN
STK FLOWRATEt DRY,STD CN
VOL OF TITRANT-SAMPLE
VOL OF TITRANT-ABS BLANK
NORMALITY OF TITRANT
TOTAL SOLUTION VOLUME
VOL SAMP ALIQUOT TITRD
CONC OF SAMPLE-STD CN


UNITS


CU.FT
DEG.R
IN^Hfi
CU.FT
DSCFM
ML
ML
G-E.Q/L.
ML
ML
LB/DSCF
PPM
LB/HR
GR/D§£F
GR/ACF
MG/NM3
KG/HR
2-1
02-20-74
S
S02 -1
66.89
547.80
28. Bl
64.72
15210.0
322.00
.05
*JJL050
210.0
40.0
^0 001 85 04
1117.9
168.9
1.2953
.8802
2964 . 0
76,60
2-1
02-20-74
5
S02 -2
66.89
547.80
28.81
64.72
15210.0
426.00
.05
.10050
160.0
40.0
.00018652
1126.8
170.2
1.3057
.8873
2987.8
77.21
2-1
02-20-74
S
H2S04
66.89
547.80
28.81
64.72
15210.0
1.60
.10
.10050
560.0
40.0
.00000352 .
13.9
3.2
.0247
.0168
56.4
1.46
2-0
02-20-74
w
S02 -1
61.43
542.90
28.81
59.93
13971.0
8.20
.05
.10050
170.0
40.0
00000410
24.7
3.4
.0287
.0228
65.6
1 .56
2-0
02-20-74
y
S02 -2
61.43
542.90
28,81
59.93
13971.0
176.00
.05
.JJLa50_
215.0
40.0
.OOOUL8J
675.5
93.7
,7827
.6223
1791.0
	 42..51_

02-20-74
W
H2S04
61.43
542.90
28.81
59.93
13971.0
18.00
.05
.10050
390.0
40.0
...QOO 03 .1.7.0
125.1
26.6
__.2219
.1764
507.7
12.05

-------
                                  AL-YSLS-DAIA
t-o
O
NAME


VM
TM
PM
VMSTD
QT
VT
VTB
N
VSOLN
VA
CS02


DESCRIPTION
DATE
PORT
POINT
SAMPLE
VOL OF DRY GAS-METER CN
AVG DRY GAS METER TEMP
AVG ARS MFTFR PRES
VOL OF DRY GAS-STD CN
STK FLOWRATE» DRY.STD CN
VOL OF TITRANT-SAMPLE
VOL OF TITRANT-ABS BLANK
NORMAI TTY OF TT.TRANT
TOTAL SOLUTION VOLUME
VOL SAMP ALIQUOT TITRD
CONG OF SAMPLE-STD CN {


UNITS


CU.FT
OEG.R
IN,HG
CU.FT
DSCFM
ML
ML
G-FQ/I
ML
ML
.B/DSCF
PPM
LB/HR
GR/DSCF -
GR/ACF
MG/NM3
KG/HR
3-1
02-20-74
S02 -1
66.77
555.90
?ft,fl7
63.79
14781.0
380.00
.04
.10050
270.0
40.0
1721.0
252.6
... L._9941_
1.3429
4563.1
114.59
3-T
02-20-74
s
S02 -2
66.77
555.90
?fl,A7
63.79
14781.0
31.00
.04
,10050
225.0
40.0
,00001934
116.9
17.2
.13*4
.0912
309.8
7.78
3-T
02-20-74
H2S04
66,77
555.90
?fl.ft7
63.79
14781.0
90.90
.04
.10050
440.0
40.0
,00017006
671.0
150.8
1.1904
.8017
2724.1
68.41
3-0
02-20-74
w
S02 -1
66.38
544.60
64.72
15211.0
70.00
.04
,100*0
200.0
40.0
,00003829
231.3
34.9
.2121
6.13.4
15.85

02-20-74
y
S02 -2
66.38
544.60
28.87
64.72
15211.0
7.00
.04
.100*0
200.0
40.0
. 000003ft!
23.0
3.5
.0267
.0211
61.0
1.58
3-0
02-20-74
H2S04
66.36
544.60
28.87
64.72
15211.0
6.00
.04
•1.0050
330.0
40.0
,J)Q 0.0.0 825
32.5
7.5
,0*77
.0457
132.1,
3.411

-------
    APPENDIX B
SAMPLE CALCULATIONS
          21

-------
                    EXAMPLE CALCULATIONS
1.  VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS


                 17.71*VM«(PB * PM/13.b)
       VMSTD *  	
                         TM*460.

                17.71* 67.06*(29.1b* 1.068/13.6)
             c  •--.—.«—•«—•—-—--«•—•--—---- s
                         75.8*460.

       VMSTM *  VMSTD«0.028317=   64.80«0.028317=


2.  VOLUME OF WATER VAPOR AT STANDARD CONDITIONS


       VWV   =  0.0474*VW  « 0.0474* 102.1      =

       VWM   *  VWV«0.028317 =  4.840*0.028317  =


3.  PERCENT MOISTURE IN STACK GAS


                  100.»VWV      100.*  4.84
       PMOS  o  •	—	*  	—	    *
                 VMSTD+VWV      64.eo*  4.8*


4.  MOLE FRACTION OF DRY STACK GAS


                 100.-PMOS       100.-  6.949
       MD    »  •««•««--•—  s  -.._.._..-___..  -c
                    100.             100.


5.  AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS

       MWD   »  (PC02 « 44/100) * (P02 * 32/100)
                    *(PN2*PCO * 28/100)

             .»  (11.0 * 44/100) * ( 3.5 * 32/100)
                    +(85.5 » 28/100)
                                                c


6.  MOLECULAR WEIGHT OF STACK GAS


       MW    «  MWD*MD + 18*(1-MD)

             »   29.9» .931 + 18*(1- .931)      »
S4.80 DSCF


 1.84 ONH3
 4.64 SCF

.1370 NM3
6.9*9 PERCENT
 .931
29.90
29.07
                            22

-------
7.  STACK GAS VELOCITY AT STACK CONDITIONS
       VS
4360*AVG SQRT(DPS«)
                4360*  17,952
                   »SQRT(1/<28.12«
       VSH   «•  VS«0.3048  •
                     29.07))

                 2737*0.3048
2737 FPM

 834 METERS/MIN
8.  STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS* DRY BASIS



                 0.123*VS*AS»MO»PS
       OS    B  .......	.....	

                      TS*460


                 0.123*  2737*  1257* .931*28.12


                         309.3 +460
                                                =     14398 DSCFM


       OSM   «  QS*0.028317 »   14398*0.028317  '»    407.71 NM3/MIN



9.  STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS



                 OS * »VMSTO
       PERI  »•• —	
                 VS*TT»PS*MD*(DN*DN)


                 1032»( 309.3*460)*   64.80
             a  .	......	...	.  a      95.8 PERCENT

                  2737* 120.0*28.12* .931* .250
                                          * .250



                               23

-------
11.   PERCENT  EXCESS  AIR  AT  SAMPLING POINT



                 100.  •  
-------
1.  Concentration of Sulfur Dioxide at Standard Conditions


      CS02 = (0.0000705) RvT-VTB) (N) (VSOLN/VA)]

                         L        VMSTD          J
                                                 230
                         [(26.10-0.10) (0.1005)  -7^
             (0.0000705)
                                      64.8


           = 0.00001635 Ib/dscf


      CPPM = (387) (CS02) (1.000.000)

                      64.06


           B (387) (16.35)

                 64.06


           = 98.8 ppm




2.  Concentration of H2S04 Mist at Standard Conditions
                                       -1
                    •      ["(VT-VTB) (N) (VSOLN/VA)
      CH2S04 = (0.000108)  -	
        CPPM
                     VMSTD

           "(0.40-0.10) (0.1005)

(0.000108)
           L          64.8

0.00000082 Ib/dscf


(387) (CH2S04) (1.000,000)

          98.08
             _ (387) (0.82)

                   98.08



             =3.2 ppm
                                25

-------
   APPENDIX C
FIELD DATA SHEETS
        26

-------
                         MIDWEST RESEARCH  INSTITUTE
                                  RUN  I—*
 MRI Project Number "5^7^ ~ C& \^
 Field Dates
 Plant
 Sampling Location  ^^/riAbbgr. "^X^Ve. f"
 Sampling Date  |c>  f
Testing Engineer   1  /yfcy/^^ //
Engr. Technician  1
                 3_

Lab Technician    1
Process Engineer   1
                 2.

Other            1
                                    FIELD CREW
                             i1
Crew Chief
MRI - Form PO  (10/72)               2?

-------
                       TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
                          Vn
PLANT __
DATE         Jj
SAMPLING LOCATION
INSIDE OF FAR WALL TO
  OUTSIDE OF NIPPLE, (DISTANCE A) _
INSIDE OF NEAR WALL TO
  OUTSIDE OF NIPPLE, (DISTANCE B) _
STACK I.D., (DISTANCE A - DISTANCE B).
NEAREST UPSTREAM DISTURBANCE 	
NEAREST DOWNSTREAM DISTURBANCE _
  CALCULATOR.

                                      <\Q"
                                                                   SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
(
z
5
1
6
Co


















FRACTION
OF STACK I.D.
























STACK I.D.
























PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1/8 INCH)
H
5?
HI
3?>4
w&
la 4


















DISTANCE B
^>6























TRAVERSE POINT LOCATION
FROM OUTSIDE OF NIPPLE
(SUM OF COLUMNS 4 & 5)
\&£ "7^
HN* // \
2*% IVfc
^^ W i
*CZ^\ ^^
<\t*rl 41±









V








EPA (Dur) 232
   4/72  •
                                             28

-------
PRELIMINARY VELOCITY TRAVERSE ,
PLANT jkatJAee VovA^er-
DATE |<3 l-e ^ "7^
LOCATION ^nA^ttf*- - ^Via.'V-
STACK I.D. 1o"
BAROMETRIC PRES
STACK GAUGE PRE
OPERATORS WAi
SURE in. Hp ^29'/"!>
SSURE. in. H-,0 ~" W . O
t

TRAVERSE
POINT
NUMBER
l-l
1_
•^
A
^
G


















AVERAGE
VELOCITY
HEAD
(Aps),in.H20
.%£•
^T)
• *\v
At
A(s
A(s




v\ \
40












A*
STACK
TEMPERATURE
(Ts), 8F
3\^
*)1~L
*>1~l
*5~l~^
^~L\
*>1L\




t'R^
^to












"5^
EPA (Our) 233
4/72
                          SCHEMATIC OF TRAVERSE POINT LAYOUT
TRAVERSE
POINT
NUMBER
























AVERAGE
VELOCITY
HEAD
(Aps), in.H20

























STACK
TEMPERATURE
(Ts), °F





















t-i. -



              29

-------
                 _      MIDWEST  RESEARCH INSTITUTE
Run Number  [ - 1              PRELIMINARY              Recorded by
Date   /<=?  7^«lb 7*f   MOISTURE DETERMINATION      Assisted by
  .A.
               NOTE: Same as Run No.
Condensor and/or Silica Gel Method
Barometric Pressure, Pg =

  D Barometer Location  	
        Reading Time	
  Q Elevation
                                                 in. Hg
                                        by

Final

Initial
Difference
Clock
Time




Dry Gas
Meter
Reading(cf)



Vm =
Flowmeter
Setting




Dry Gas
Meter
Temp (°F)




Impinger
Water Volume
(ml)



Wc =
Tube No.


Weight (Grams)
Final


Initial


Total Moisture Adsorbed'.
Di fference


Wa =
        Meter Pressure,   Pg ** Pm
        Average Meter Temperature,  Tm
        Total Weight of Moisture
          Collected, We + Wa = Wm
                                                        in. Hg
                                                        OF
      Moisture Content =
                                100
                                                        gm

                                                        % by Volume
                        I + 375
                                PmVm
                              (Tm+460) Wm
   B.  Wet/Dry Bulb Method
              Dry Bulb Temperature
              Wet Bulb Temperature

      Moisture Content (from Ref. Table)

   C. Predetermined Value

              % Moisture      /
                                                 °F
                                                 °F
                                                 % by Volume
                              Basis
 MRI - Form P4 (10/72)
                                        30

-------
                                  NOMOGRAPH DATA
I  IsO
           PLANT.

           DATE_
           SAMPLING LOCATION
t/ 6 r"Vt fc> C?
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE IVIETER TEMPERATURE (AMBIENT + 20 °F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
T|navg.
Bwo
V
ps
PVP
/rm
savg.
APavg.
APmax.
I,M
10
1
29,1^
-Wu1
\°>(^
^0
AO
4 1/
, vz
,rc)
.75
w
          EPA (Our) 234
             4/72
                                    31

-------
                                               DRY MOLECULAR WEIGHT DETERMINATION
      PLANT.
      DATE
                                 V;
COMMENTS:
      SAMPLING TIME (24-hr CLOCK).
      SAMPLING LOCATION	
      SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
      ANALYTICAL METHOD	
      AMBIENT TEMPERATURE	,	
      OPERATOR	
\^ RUN
GAS ^^\
C02
02 (NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N£ (NET IS 100 MINUS
ACTUAL CO READING)
1
.ACTUAL
READING




NET




2
ACTUAL
READING




NET




3
ACTUAL
READING




NET




AVERAGE
NET
VOLUME

Vi



MULTIPLIER
44/100
1 	 ~
32/100
. i
a/ioo
a/MO
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole




TOTAL
CO
ro
      EPA (Dur) 230
        4/72

-------
                                                                FIELD DATA
u>

TRAVERSE
POINT
NUMBER


•5-1
~
•
A
I

1
,2
^
*M
/9
^


4
5
*f
£,
to











PLANT ^/K«LiM**» KX-UO-
DATE K9 T=eb ~K
SAMPLING Lf
SAMPLE TYP
RUN NUMBEF
OPERATOR
AMBIENT TEI
BAROMETRIC
STATIC PRE
FILTER HUM
\. CLOCK TIME
75 — — -J332











&*>**>











TCATION 5^-J-lxkbor- J/V leT
F t>0^
j-T
Ad A.
MPFRATURF *\.*59
PRFSSURF "Zl^D. l<3
.SURF (P i — /4.O
RFR U)
PROBE LENGTH AND TYPE J ~4r*TC* &L4S>
NOZZLE ID I 2.


ASSUMED MC
SAMPLE BO
METER BOX
METER AHS
C FACTOR
^* /
1ISTURF «. ~7
K NUMBER II
NUMBER ^>

,e^T_
PROBE HEATER SETTING
HEATER BOX SETTING

SCHEMATIC OF TRAVERSE P
READ AND RECORD ALL DATA EVERY
GAS METER READING
(V ) fp
*"1CT Q. *^ ^L
I ^ C7* 1 »«
"lkO(r
Tip^.^^
"7(^« ^T
ifc^^-j
liz..^
T~lfl",^2,
• l™7 .^ j^l
Tfipi tV^
•7^3.^1
")^.33)
7^.20)
"107.7^











VELOCITY
HEAD
(ApJ, in. HiO
•"55
• V/
,^^H
^<5
A \
•Ml
^1 ^
f\^7
4v
' ^-=>
^j C^.
£\ T











ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H20)
DESIRED
,91
•93
i,i^
/.ic/
!.
i.oa
/.o<9
Lo<)
(>(5
'vi*5
/.ra
l-'Z-l











ACTUAL























DINT LAYOUT
S MINIIT

STACK
TEMPERATURE
(TS).°F
5tZo
Siu»
^i<5
5l^4
3\u»
31**
^ It
5l^\
^HS
Sv5







(



REFERENCE
ES
_|
^*:>
^^//P
£^ *1
^&
"5
51

<^Z.
^"5
64
(*&
G?l
O B











PUMP
VACUUM.
in. Hg
&
g
s
9
«^
?,*5
^)iS
«^^
1^
f«?
M
II











SAMPLE BOX
TEMPERATURE.
°F
3."5o
*3. t*l
J?*51
-2"^H
5lo
2^o
2 VA
Z3o
21-3
,2<5«5
-?&J
^d3












IMPINGER
TEMPERATURE.
°F

Ceo

G»S

TD

















COMMENTS:
EPA (Dur> 235
4 72

-------
 TRAVERSE
   POINT
  NUMBER
                                   GAS METER READING
 VELOCITY
   HEAD
api  in. H0
ORIFICE PRESSURE
 DIFFERENTIAL
  lAHi. in  H^O)
                                                                    DESIRED  ACTUAL
   STACK
TEMPERATURE
  iT$i.0F
DRY GAS METER
TEMPERATURE
                                                                                                   INLET    OUTLET
 PUMP
VACUUM.
 in HI
 SAMPLE BOX
TEMPERATURE.
      °F
  IMPINGER
TEMPERATURE
     °F
                                                                                                            01
                                                                                                                      S.5
                                                                                                                                               IS
                                       8/ 1 »  65
                                              . a.
                                                                                                      &
                                                                    ,6
EPA (Dur) 236
  472

-------
                         MIDWEST RESEARCH  INSTITUTE
 MRI Project Number
 Field Dotes
 Sompling Location
 Sampling Date  \c>>
Crew Chief
Testing Engineer   1
                 l_
                 3
Engr. Technician  1
                 2_
                 3
Lob Technician
                2_
                3
Process Engineer  J_
                2
Other           ]_
                2
                                  RUN
                                   FIELD CREW
      \
MRI - Form PO  (10/72)
                                       35

-------
                       TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
PLANT 	
DATE . /9
SAMPLING LOCATION
INSIDE OF FAR WALL TO
  OUTSIDE OF NIPPLE, (DISTANCE A) _
INSIDE OF NEAR WALL TO
  OUTSIDE OF NIPPLE, (DISTANCE B) _
STACK I.D., (DISTANCE A - DISTANCE B).
NEAREST UPSTREAM DISTURBANCE	
NEAREST DOWNSTREAM DISTURBANCE
CALCULATOR.
                                 -7
                                                                     SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
1
z
3
1
1
(/


















FRACTION
OF STACK I.D.
,044
i/n
,Z^5
ao-5T
• 6-53
,0^


















STACK I.D.
^lo"























PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1/8 INCH)
\^ \\
^•66 ^ 5
ll.&o /li
Zg.eo *?&i
M.lt VI -i
3&.Z^ ^25


















DISTANCE B
fri























TRAVERSE POINT LOCATION
FROM OUTSIDE OF NIPPLE
(SUM OF COLUMNS 4 & 5)
IcM
14*
201
^G?^
4Zt
^1(^1











•'






EPA (Dur) 232
   4/72
                                                   36

-------
PRELIMINARY VELOCITY TRAVERSE
PLANT _J
DATE	«2
LOCATION
STACK I.D..
BAROMETRIC PRESSURE, in. Hg.
STACK GAUGE PRESSURE, in. H,0.
OPERATORS.
                             SCHEMATIC OF TRAVERSE POINT LAYOUT
TRAVERSE
POINT
NUMBER
i .
^
,
4
r
' £'











• . •






AVERAGE
VELOCITY
HEAD
(Aps), in.^O
' 3 (?
3> )
< "^ "7
. c;
r?
, C/v


















• y 3
STACK
TEMPERATURE
. °F
























^J^
EPA (Out) 233
4/72
TRAVERSE
POINT
NUMBER
























AVERAGE
VELOCITY
HEAD
(Aps), in.H20

























STACK
TEMPERATURE
(TS). °F

























                  37

-------
Run Number
Dote  JO)
                MIDWEST RESEARCH  INSTITUTE
                         PRELIMINARY              Recorded by
                  MOISTURE DETERMINATION      Assisted by
  .A.
               NOTE; Same as Run No.
Condenser and/or Silica Gel Method
Barometric Pressure, Pg  =

  D Barometer Location  	
        Reading Time
  P Elevation
                                                 in. Hg
                                       by

Final

Initial
Difference
Clock
Time




Dry Gas
Meter
Reading(cf)



Vm =
Flowmeter
Setting




Dry Gas
Meter
Temp(°F)




Impinger
Water Volume
(ml)



Wc =
Tube No.


Weight (Grams)
Fi na 1


Initial


Total Moisture Adsorbed'
Difference


Wa =
        Meter Pressure,   Pg "*& Pm
        Average Meter Temperature,  Tm
        Total Weight of Moisture
          Collected, We + Wa = Wm
                                                        in. Hg
                                                        OF
      Moisture Content =
                                JOO
                                                        gm

                                                        % by Volume
                        I + 375
                                PmVm
                              (Tm+460) Wm
   B.  Wet/Dry Bulb Method
              Dry Bulb Temperature          :
              Wet Bulb Temperature          :

      Moisture Content (from Ref. Table)

   C. Predetermined Value

              % Moisture     AQ [t)   Basis
                                                 °F
                                                 '°F
                                                 % by Volume
                                           iL ^i?X
 MRI - Form P4 (10/72)
                                     38

-------
PLANT

DATE
s\<
 SAMPLING LOCATION
                        NOMOGRAPH DATA

                        *0
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in; H20
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
T|navg.
Bwo
Pm
ps
V
/rm
savg.
APavg.
APmax.
!>?<•/
o
70
^,0 %
^~S? £2 a
'• 1 £-
•*-£-&&.

i>
-------
                                         DRY MOLECULAR WEIGHT DETERMINATION
PLANT.
DATE_
                                                                  COMMENTS:
                       7*1
 SAMPLING TIME (24-hr CLOCK).
 SAMPLING LOCATION	
 SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
 ANALYTICAL METHOD	
 AMBIENT TEMPERATURE	
 OPERATOR     	
^^ RUN
GAS ^^\
C02
02(NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N 2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING




NET




2
ACTUAL
READING




NET




3
ACTUAL
READING




NET




AVERAGE
NET
VOLUME

3-5
O.o


MULTIPLIER
44/100
!
32/100
a/ioo
a/ioo
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole




TOTAL
EPA (Dur) 230
   4/72

-------
75 9,
                                                                                      FIELD DATA
                                     PLAHT
                                     DATE
                                     SAMPLING LOCATION _^=^
                                     SAMPLE TYPE .
                                     RUN NUMBER _
                                     OPERATOR	
                                                                                   PROBE LENGTH AND TYPE
                                                                                   NOZZLE I.D.    ' l.,,\-~''
                                                                                   ASSUMED MOISTURE.'.	
                                                                                   SAMPLE BOX NUMBER	
                                                                                   METER BOX NUMBER	
                                                                                   METER
                                                                                                                                       ) "
       AMBIENT TEMPERATURE
       BAROMETRIC PRESSURE _
       STATIC PRESSURE, (P^)    —
       FILTER NUMBER (s)	
                                                                                                                       "g-
                                                                                                                CFACTOR.
                                                                                                                PROBE HEATER SETTING.
                                                                                                                HEATER BOX SETTING	
                                                                                                                REFERENCE Ap	
                                                                              SCHEMATIC OF TRAVERSE POINT LAYOUT
                                                                       READ AND RECORD ALL DATA FVFRY   *5   MINUTES
                 TRAVERSE
                  POINT
                  NUMBER
                                    CLOCK TIME
                     GAS METER READING
                          (V). It3
                VELOCITY
                  HEAD
               Ups). in. H20
ORIFICE PRESSURE
  DIFFERENTIAL
  (AH), in. H20)
                                                                                   DESIRED   ACTUAL
   STACK
TEMPERATURE
  (T$)."F
DRY GAS METER
TEMPERATURE
                                                                                                                  INLET
                                                                                             OUTLET
 PUMP
VACUUM.
 in. Hg
 SAMPLE BOX
TEMPERATURE.
      °F
  IMPINGER
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      °F
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         EPA (Dm) 236
            472

-------
                         MIDWEST  RESEARCH  INSTITUTE
MRI Project Number
Field Dat
Plant
Sampling Location
Sampling Date ^
Crew Chief
Testing Engineer  1
Engr. Technician 1_
Lab Technician
Process Engineer  1
                2

Other           1
                                 RUN
                                   FjELDCREW
MRI - FormPO  (10/72)
                                        43

-------
                        NOMOGRAPH DATA
 PLANT

 DATE_
 SAMPLING LOCATION
                                                 r-7
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20 °F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap. in. H20
AH@
Tmavg.
Bwo
Pn,
ps
Ps/Pm
savg.
APavg.
APmax.













EPA (Dur) 234
   4/72
                               44

-------
      PLANT.
JX&
V:
                                               DRY MOLECULAR WEIGHT DETERMINATION
                                       COMMENTS:
      SAMPLING TIME (24-hr CLOCK).
      SAMPLING LOCATION	
      SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
      ANALYTICAL METHOD	
      AMBIENT TEMPERATURE	
      OPERATOR	
\^ RUN
GAS ^"\^
C02
O£(NET is ACTUAL o2
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
^2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING




NET




2
ACTUAL
READING




NET




3
ACTUAL
READING




NET




AVERAGE
NET
VOLUME

3.5
0,-a


MULTIPLIER
44/100

I: 	
32/100
_ i
a/ioo
^/lOO
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole




TOTAL
Ui
      EPA (Dur) 230
        4/72

-------
                           yjyt^/wtuc
                                                                     FIELD DATA
                     PLANT.
                     DATE
                     SAMPLING LOCATION
                     SAMPLE TYPE
                     RUN NUMBER.
                     OPERATOR _£
                                                                                               PROBE LENGTH AND TYPE
                                                                                               NOZZLE 1.0.
                                          rr
                    AMBIENT TEMPERATURE
                    BAROMETRIC PRESSURE .
                    STATIC PRESSURE, (Ps) __T_
                    FILTER NUMBER Is)	
                                                             ASSUMED MOISTURE.'.	i
                                                             SAMPLE BOX NUMBER     A Z-
                                                             METER BOX NUMBER     "b
                                                             METER AHg
                                                             C FACTOR	
                                                                                                PROBE HEATER SETTING.
                                                                                                HEATER BOX SETTING	
                                                                                                REFERENCE An	
                                                             SCHEMATIC OF TRAVERSE POINT LAYOUT
                                                       READ AND RECORD ALL DATA EVERY
                                                                                          MINUTES
TRAVERSE
 POINT
 NUMBER
           SAMPLING 1
            TIME.min
                    CLOCK TIME

                          2h'
GAS METER READING
     og. it3
 VELOCITY
   HEAD
(APS), in. H20
ORIFICE PRESSURE
 DIFFERENTIAL
  (AH), in. H20)
                                                                   DESIRED   ACTUAL
   STACK
TEMPERATURE
  (TS).°F
DRY GAS METER
TEMPERATURE
                                                                                                 INLET
                                                                                                (To, jn),°F
                                                                                                           OUTLET
 PUMP
VACUUM.
 in. Hg
 SAMPLE BOX
TEMPERATURE.
      °F
  IMPINGER
TEMPERATURE.
     "F
                                                      .37
                                                                                                                     1(7
                                                                  1.12,
    'S
                                                                    1.1
                                                                                                   (0(7
                                                                                                   141
                                                                   I.Z.S
                                                                                                    (oz.
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    (6
                                                                             l.c?
COMMENTS:

EPA (Our) 235
   472
                                                                        U

-------
'-'9
i.o
I.C5
f/x    0..4-
              1,5   21)
270
63
                      23-7
       «> 3

-------
                         MIDWEST  RESEARCH INSTITUTE
MRI Project Number
Field  Dotes
Plant   :3
           &  r^, t -e
Sampling Location   /^)JJ
Sampling Date  ^L
Crew Chief
Testing Engineer  1
Lab Technician
Process Engineer   1
Other
J_
2
Engr. Technician 1     l^hi I
                                   FIELD CREW
MRI - Form PO  (10/72)
                                   ' 48

-------
                        NOMOGRAPH DATA
  PLANT.

  DATE_
 SAMPLING LOCATION
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20°F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR '
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@ •
T|t1avg.
Bwo
rm
PS :'
PS/Pm '
savg.
^Pavg.
^Pniax.













EPA (Our) 234
   4/72
                                  49

-------
          PLANT.
          DATE.
                                                   DRY MOLECULAR WEIGHT DETERMINATION
COMMENTS:
          SAMPLING TIME (24-hr CLOCK).
          SAMPLING LOCATION.	
          SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
          ANALYTICAL METHOD _-	
          AMBIENT TEMPERATURE	:	
          OPERATOR	
\^ RUN
GAS ^\^
C02
02(NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N£ (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING




NET




2
ACTUAL
READING




NET




3
ACTUAL
READING




NET




AVERAGE
NET
VOLUME

^


-
MULTIPLIER
44/100
1
32/100
^/lOO
K/m
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole




TOTAL
Ln
O
         EPA (Dur) 230
            4/72

-------
FIELD DATA

PLANT 2> na^^tf
DATE _? /JL*/ Tt,/


SAMPLING LOCATION ,-„ ,«-/ W

SAMPLE TYP
RUN NUMBER
OPERATOR
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AMBIENT TEMPERATURE **&

TRAVERSE
POINT
NUMBER
/

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 1
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GTH AND TYJ
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ISTURE,'.
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NUMBER


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SCHEMATIC OF TRAVERSE P(
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IVm). It3
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EPA (Dur) 236
   4/72

-------
                         MIDWEST  RESEARCH  INSTITUTE
MRI Project Number
Field  Dates
Plant
                       ^f

Testing Engineer   1  /^/<
Engr. Technician  1
Lab Technician    1
Process Engineer   1
Other            1
                2
                                  RUN     ,—
Sampling Location      	
Sampling Date  £2.o'7^^ fe,"-?	

                                   FIELD CREW

Crew Chief
MRI - Form PO  (10/72)
                                       53

-------
  PLANT

  DATE_
        ""

                        NOMOGRAPH DATA
  SAMPLING LOCATION
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20°F), °F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
Tmavg.
Bwo
pm
Ps
V
/rm
savg.
A.Pavg.
APmax.













EPA (Dur) 234
   4/72
                                 54

-------
                                                  DRY MOLECULAR WEIGHT DETERMINATION
PLANT.
DATE.
                                                                          COMMENTS:
         SAMPLING TIME (24-hr CLOCK).
         SAMPLING LOCATION	
         SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
         ANALYTICAL METHOD	
         AMBIENT TEMPERATURE	
         OPERATOR
^. RUN
GAS ^\
C02
02 (NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N£ (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING



..
NET




2
ACTUAL
READING




NET




3
ACTUAL
READING




NET




AVERAGE
NET
VOLUME

S
4) *?


• v
MULTIPLIER
44/100
f
32/100
_ _ 1
a/iob
a/wo
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Mj, Ib/lb-mole
-



TOTAL
Ln
Ui
        EPA (Dur) 230
           4/72

-------
                     PLANT.
                     DATE'_
                                                                    FIELD DATA
                                      TH
                                                                           PROBE LENGTH AND TYPE
                                                                           NOZZLE I.D	i 2
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE   *? •?
BAROMETRIC PRESSURE
STATIC PRESSURE. (Pj^-
FILTER NUMBER (s)	
                                                                                               ASSUMED MOISTURE.'. _
                                                                                               SAMPLE BOX NUMBER _
                                                                                               METER BOX NUMBER     "b
                                                                                               METER AHg       i . *
                                                                                               C FACTOR '_	. O
                                                                                                                    72-
                                                                                              PROBE HEATER SETTING.
                                                                                              HEATER BOX SETTING	
                                                                                              REFERENCE ap	(_
                                                            SCHEMATIC OF TRAVERSE POINT LAYOUT
                                                     READ AND RECORD ALL DATA EVERY.
                                                                      MINUTES
TRAVERSE
 POINT
 NUMBER
                   CLOCK TIME
              GAS METER READING
                   (Vm). 1(3
                                                        VELOCITY
                                                          HEAD
                                                       IAps). in. H20
ORIFICE PRESSURE
  DIFFERENTIAL
  (AH), in. H20)
                                                                 DESIRED   ACTUAL
   STACK
TEMPERATURE
  
-------
TRAVERSE
 POINT
 NUMBER
           TIME
                                                                                                   INLET
                                                                                                             OUTLET
                    CLOCK TIME
                                    GAS METER REAOING
                                         'V ^
VELOCITY
  HEAD
ORIFICE PRESSURE
  DIFFERENTIAL
  IAH). in HOi
   STACK
TEMPERATURE
  lT$i.°F
DRY GAS METER
TEMPERATURE
 PUMP
VACUUM.
 in HS
 SAMPLE BOX
TEMPERATURE.
      •F
  IMPINGER
TEMPERATURE
      °F
                                                                                                    loB
                                                                    MT
                                                                                                   r/c
EPA (Dur) 236
  472
                                                                     ,<

-------
                         MIDWEST  RESEARCH INSTITUTE
MRI Project Number
Field Dates
Plant
                        cj
Sampling Location^
Sampling Date
Crew Chief
Testing Engineer  1
                2
                3

Engr. Technician 1
                2
                3
Lab Technician
                2.
                3
Process Engineer  1
                2~
Other           ]_
                2
                                 RUN
                                   FIELDCREW
MRI - Form PO  (10/72)
                                   58

-------
 PLANT
                        NOMOGRAPH DATA
 DATE.
 SAMPLING LOCATION
/
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20 °F),°F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in. Hg
STATIC PRESSURE IN STACK, in. Hg
(Pm±0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, °F
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap, in. H20
AH@
Tmavg.
Bwo
Pm
ps
Ps/Pm
savg.
*Pavg.
APmax.













EPA (Our) 234
   4/72
                              59

-------
                                         DRY MOLECULAR WEIGHT DETERMINATION
                                                                 COMMENTS:
 SAMPLING TIME (24-hr CLOCK).
 SAMPLING LOCATION	
 SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
 ANALYTICAL METHOD	
 AMBIENT TEMPERATURE	
 OPERATOR      '	
U(j
\«. RUN
GAS >\
C02
02(NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO (NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N 2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING




NET




2
ACTUAL
READING




NET




3
ACTUAL
READING




NET




AVERAGE
NET
VOLUME

\f



MULTIPLIER
44/100
i "
32/100
— — 1
a/100
a/wo
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole




TOTAL
EPA (Dur) 230
   4/72

-------

 TRAVERSE
   POINT
  NUMBER
   GAS METER READING
            3
                                             Ll
 VELOCITY
   HEAD
tilpjl in. HjO
ORIFICE PRESSURE
 DIFFERENTIAL
  lAHUn HjO)
                                                                 DESIRED  ACTUAL
   STACK
TEMPERATURE
  (T$I.°F
DRY GAS METER
TEMPERATURE
                                                                                              INLET    OUTLET
 PUMP
VACUUM.
 in H|
                                                                                 i£-
 SAMPLE BOX
TEMPERATURE.
     °F
  IMPINGER
TEMPERATURE.
              c
                               •4-
     .-f  -
                                                                 ^-0+
                                                                                                                10
                                  ^£-
                                                                                               677
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