Report No. 76-ARM-11
  CD

<^
O
        POLLUTIO
EMISSION  TEST
                     Visible Emissions
                     Elk Roofing Corp.
                     Stephens, Arkansas
          UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
                Office of Air and Waste Management
              Office of Air Quality Planning and Standards
                  Emission Measurement Branch
               Research Triangle Park. North Carolina

-------
VISIBLE EMISSION MEASUREMENT AT ASPHALT ROOFING PLANTS
           EMB Project Report No. 76-ARM-ll
                     Plant Tested
                Elk Roofing Corporation
                  Stephens, Arkansas
                 August 19 - 21, 1975
                     Prepared for
            Environmental Protection Agency
               Emission Measurement Branch
                 Research Triangle Park
                 North Carolina   27711
                   W. R. Feairheller
                     T. L. Stewart
             Monsanto  Research  Corporation
                   Dayton Laboratory
                   1515 Nicholas  Road
                   Dayton, Ohio
           Report  Reviewed by  J.ohn W.  Brown

          Contract  No.  68-02-1404, Task No.

-------
                        TABLE OP CONTENTS


                                                        Pag.e
 I.   Introduction                                         1

II.   Summary and Discussion of Results                    3


Appendix  Field Data Sheets

-------
                        I.   INTRODUCTION

Under the Clean Air Act, as amended, the Environmental Pro-
tection Agency is charged with the establishment of perfor-
mance standards for new installations or modifications of
existing installations in stationary source categories which
may contribute significantly to' air pollution.  A performance
standard is a standard for emissions of air pollutants which
reflects the best emission reduction systems that have been
adequately demonstrated (taking into account economic consider-
ations) .

The development of realistic performance standards requires
accurate data on pollutant emissions within the various source
categories.  This report presents the results of the testing
which was performed at the Elk Roofing Corporation Plant in
Stephens, Arkansas on August 19-21, 1975.

Monsanto Research Corporation as a contractor to the Environ-
mental Protection Agency under the "Field Sampling of Atmos-
pheric Emissions" program was requested to provide visible
emission data from the Elk Roofing Corporation.

The field testing program was under the direction of John W.
Brown, Field Testing Section, Emission Measurement Branch, EPA,
The visible emissions were observed and recorded by Tommy L.
Stewart, observer #1, and Charles F. Duncan, observer #2, of
Monsanto Research Corporation.
                                1

-------
There are two blowing stills at this plant.  Each still has
a knockout box to remove heavy materials.  The emissions from
the knockout boxes are combined and ducted to an afterburner
and heat exchanger and are then ducted to the atmosphere
through a 30 foot stack.  Visible emission data were recorded
on the effluent from this stack, for a period of about four-
teen and one half hours-. . During the observation period there
were no major mechanical problems and the process was con-
sidered to be typical of normal operation.

The visible emissions were determined as prescribed by EPA
Method 9 as given in the Federal Register, Vol. 39, No. 219,
November 12, 1974.  Opacity readings were made from three
locations within the plant site so that the angle with the
line of observation and the sun would be no more than seventy
degrees.  This report presents a summary of the visible emis-
sion data and all field data sheets are included in the ap-
pendix.

During the same periods in which visible emissions were being
observed, personnel from Battelle Memorial Institute (Columbus,
Ohio) were conducting sampling of the emissions of particulate
(Method 5)5 S02 (Method 6), gaseous hydrocarbons, and polycyclic
organic materials.  This information is presented in a separate
report under the same EMB Project Report No. (76-ARM-ll).

-------
             II.   SUMMARY AND DISCUSSION OF RESULTS

.The visible emission data was recorded for a total of about
fourteen and one half hours over a three day period, at
fifteen second intervals as specified by Method 9.  Observer
Tommy L. Stewart was certified by the Environmental Protection
Agency of the State of Ohio in Columbus, Ohio on March 27,
1975.  Observer Charles P. Duncan was recertified at the EPA
Air Pollution Training Institute Visible Emissions Recertifi-
cation course given in Kansas City, Missouri on August 4-6,
1975-

During the entire observation period, the percent opacity
was recorded at Q%, that is, no visible emission could be
detected.

The physical layout of the plant showing the location of the
stills, afterburner and heat exchanger as well as the loca-
tion of observation points and direction of observation are
shown in Figure 1.  A summary of the time of observation,
observation point used, pertinent distances, weather condi-
tions and opacity is presented in Table 1.  The plot of
observed opacity against elapsed observation time is given
in Figure 2.  The summaries of visible emissions for each
observer's readings are included following Figure 2.

-------
                                       N
                           approximate observers
                                  position
  Observers #1 and #2 positions were between  these
  points, 50-80 feet from the stack.  For  exact
  locations, see Table 1.

Figure 1.   Position of Observers Reading  Visible
            Emissions

-------
                              Table 1.    SUMMARY OP VISIBLE EMISSION DATA
                                         ELK ROOFING CO.,  STEPHENS, ARKANSAS
VJ1

Date
8-19


8-19

8-19

8-19

8-20

8-20

8-20

8-20

8-21
8-21


8-21

8-21

21 Hr. Clock
Time
12:17-17:02


12:17-17:02

17:12-18:29

17:12-18:29

13=33-15:09

13:33-15:09

15:56-17:28

15=56-17:28

10:08-11:18
10:08-11:18


13:11-17:52

13:11-17:52

Wind
Dist. to Direction Wind Velocity
Observer Source (ft) from Source Direction MPH
1 50-60 E - S.E. E - S 5-10


2 50-60 E - S.E. S 8-12

1 50-60 E S - N.E. 5-10

2 50 S.E. S - N 5-10

1 50-60 S.E. S - S.W. 8-20

2 50 S.E. N - S 8-15

1 60 E S 5-10

2 50 S.E. S.W. - N.E. 8-12

1 60 E N - E 8-12
2 60 E N.E. - S.W. 8-12


1 50-80 E - S.E. N.E. 8-12

2 15-80 S.E. - S.S.E. N.E. - S.W. 5-12


Weather
Part
Cloudy
(30?)
Part
Cloudy
Part
Cloudy
Part
Cloudy
Part
Cloudy
Part
.Cloudy
Part
Cloudy
Part
Cloudy
Clear
Clear-
Part
Cloudy
Part
Cloudy
Part
Cloudy

Background
Sky


Sky

Sky

Sky

Sky

Sky

Sky

Sky

Sky
Sky


Sky

Sky



Time-Opacity
213


215

78

78

97

97

93

93

100
100


258

258

mln 30 sec-OZ


min 30 sec-0/8

min - 0%

min - 0%

min - 0$

min - 0%

min - '0%

mln - 0%

min 30 sec-0?
min 30. sec-OZ


min - 0%

min - 0?

      Observer #1 - Tommy Stewart

      Observer #2 - Chuck Duncan

-------
     20'
     15-
Q_
O
     5-
      0
                             6       8       10
                               TIME (HOURS)
12    '- 14      16
                       Figure 2.  Opacity Plot

-------
7>pt of
Type of Discharge: &C/



Location of Discharge:



Height of Point of Discharge:-^?'



Description of Background:



Description of Sky:



Wind Direction:



Color of Plume: y



Duration of Observation:



              SUtfi-iARY OF AVERAGE OPACITY
.Distance  from Observer to Discharge



 Height  of Observation  Point: f4e*^~sf+*•



 Direction of Observer  from Discharge  Point:
 Hind  Velocity:   5"



 Detached  Plume:
                SUMMARY OF AVERAGE OPACITY
Time • Opacity lime Opacity
Set Number- Start End Sum Averaoe Set Number Start End Sum Aver<
. * "^
1 /£*/ )Z'$3 0 0 ' 21 W 'f^ C
2 /2:$3 ll'13-Z3.
•1 ry.2'3 i3'Zi
3 • /3-2? i3'3$
"9 >3:3* tf'.fr
10 /?;*/ /rfo
'' ;-'l:^7 /3^5?
' >2 /3-53 i3'-5<7
'3 /'?;59 iL/rf,<
, . / J'3/ 14 -O 3
J4 • t'-/'~cS its-,/
ic 3 ' T ' //
lb ^-// /^;/7
16 /^''7 /V:2J
^7 'V '^ /V = 2^
^8 /V-'?f /^:35
19 /y:5$* ;v-V/
20 /V;V/ '/vr^7 \



















' 1

?? .... /v-<5^ /y^/
«- L. , _ /— ^j. *-,, , O
oo ;^-5f /^.<^3
'•^ ;C .>«' ,C 1 1
2d r'5'^5 /5
27 /6;--'? ^-35
*- ° . _ / <~ ' /, i
29 /3-/5r °'^/
30 /t>'.-^/ /o':'47
31 /5V'!<7 -/5V 53
32 - . /5-VJ '5-Vy
33 y^-'i-"? /6- o
















•

' N
                                                V3

-------
                              ,
-------
/ L)3 tP '
                                      01
                                                  [.missions
  Type-  of
 Type  of  Discharge:

 Location of  C
 *
 Height of Point of Discharge:

 Description  of Background:

 Description  of Sky:
                                                                                       .- 0
                                             Distance from Observer to Discharge

                                             Height, of Observation Point

                                             Direction of Observer from Discharge  Point:
                        S~ ^—
                                <7
Wind Direction:

Color of Plume:

Duration of

              SUMMARY OF AVERAGE OPACITY
Wind Velocity:  $"-/*

Detached Plume:
                                                             SUMMARY OF AVERAGE OPACITY
Tune Opacity Time Opacity
Set Number
1
2
3
4
5
6
7
8 •
•9
10
11
• 12
13
1A
4
15
1c_
6
17
18
19
20
btart End Surn^ Average ' Set Number Start End Sum Average
17' /Z 17: It 0 0 ' 21
/7-/fr rt,Z " £ '// » f\ / ^ fr II M
*"*r j *) Q
— j X i ^, ^ /) /•* tt It ^~ Q
/ tx- ^n / j|^ / w K^ / * f i •
/*.'** ' > i, 29
rf'.olf /r^y )( 1(' 30
(%-ji, /v'^V » " 31
/? '/y V , ^7 M 32
— _ " — _^^ • 	 • * O O
/*^3^ -j-f,3tr - 24
/J-& T^rnrr 35
•^ -"~~~ 36
37 ' .
38
39 ...
40

-------
       :/ I C Llli . _, .
 Date:  /)b
 T>pc- of Pi
 Type of Discharge:
 Location of Discharge:
"height of Point of Discharge:
 Description of Background: i
 Description of Sky:
 .Wind Direction:  V
 Color of Plume: /Lt
 Duration of Observation:  f~7/2-
                SUMMARY OF AVERAGE OPACITY
                                                   X
       Distance from Observer to Discharge Point:.**'
a*r**r Height of Observation Point: 6.*0't£*'f<.
       Direction of Observer from Discharge PointrSff
       Wind Velocity:
       Detached  Plume:
                       SUMMARY  OF AVERAGE  OPACITY

Set Number
1
2
3
4
5
6
7
8 •
'9
10
11
• 12
U
14
15
16
17
18
19
20 -
nme •
Start
/7/Z
/7/ffi
i?Zif
/>1f^
(&oo
l&M
tSf*-
Ifffe
/fiZt
/#?o







Opacity
Sum
0
O
D
O
0
O
0
O
O
O
O
O
0







Average
O
O
O
0
0
O
0
O
O
O
O
O
O








Set Number
r*
' 21
22
23
2.4
25
26
27
28
29 '
30
31
32
33
34
35
36
.37
38
39
40
1 i rns
Start




















End













.






Opacity
Sum




















Average





















-------
                              Summary  of  Vis;!;1 admissions
                                            ^   -i-
Date:
Typt of
Type of Discharge:
Location of C
Height of Point of Discharge:
Description of Background:
Description o-f Sky:
Wind Direction:  $^<$// _ 5
Color of Plume: #£/1£4&&
Duration of Observation:/yU
              SUMMARY OF AVERAGE OPACITY
                                             Distance from Observer'to Discharge Point:
                                             Height of Observation Point
                                             Direction of Observer from Discharge
                                             Hind  Velocity:  fr-fZO
                                             Detached  Plume:  •  .
                                                            SUMMARY OF AVERAGE OPACITY
Time Opacity Time
Set Number Start End Sum Average Set Number Start End
•?- D @
2 /5'39 '3'VtT
3 '3~V5 '?:5/
4 /3;5/ /2:57
5 '3-J7 t27 W'-_&
•• ] 2 1^' *$ H" 3 \













\
F
22
23
24
25
26
27
28
29 •
30
31
32
33
34
35
36
17 /5 '^3 I5'f>9 37
18 38
19 .39
20 . ' 40
Opacity
Sum Average





















-------
                                       i-ACIL-  Y
                              Sun;:;;ary of Visile  Emissions
                              S _~i r- f— ft-, i. I I'— rf-*^ \_1.
                                                                    £'/-/    /
Date: five.  20 j I
Type of Plant: ASPHALT
Type of Discharge:  STAC/r                 Distance  from Observer  to  Discharge Point:
Location of Discharge: B^WfC. Sr/u. 'Our iejr Height of Observation Point: •?
?3&
/If?
/•&of
.
nr.?..
ItyoJ
JLfofy
/*f-/'>~ /y?-/
/J
o o
o
IT/0 \ 0








o
o



\
' 21
22
23
24
25
26
27 1
28








29
30
31


32 • i
33 .
34
35
36
37
38





39 !
40








































Average
—







•











-------
                              Summary of Visile Emissions
uote:
     of
Type of Discharge:
Location of Di
Height of Point of Discharge:
Description of Background:.
Description of Sky:
Wind Direction:
Color of Plume: /Z
Duration of Observation:
              SUMMARY OF AVERAGE OPACITY
                                            Distance from Observer to Discharge
                                            Height, of Observation Point: ^u»^^
                                            Direction of Observer from Discharge  Point
                                            Wind Velocity:
                                            Detached Plume:
                                                           jr-xr
                                                           SUMMARY OF AVERAGE OPACITY
Time • Opacity Time Opacity
Set Number Start End Sum Average Set Number Start End Sum Average
! /5;56> MoZ I
2 Jb'dZ. ib'0%
3 }(>'6% )&>32 iie^Sfr
8 • lii''5jr lu'tyy
. '9 ib^Hy lif'f'jO
10 H»'$o / $(* n~'0i.
•12 /7:oz, /?,
-------
Sui;,;;;jry of VI   ole  Emissions-
3c> F
Date: ftuG- 2&

Type- of Plant: ft$PHALT

Type of Discharge:  S

Location of Discharge:

Height of Point of Discharge:

Description of Background:

Description of Sky:

Wind Direction:

Color of Plume:  A/7~
                              SUMMARY OF AVERAGE OPACITY
Time ' Opacity
Set Number Start End Sum
1
.._
3
. 4 . .
5
6
•7
8 •
•9
IP _
11
12
!
SfJ~6 /6&2- £>
(&OZ- /&O8 O
/<^/V /<£20 i O
/<^2o /^2-^ 1 &
}£iC fa-$1_ O
~'ici'& &Q(f '• &
faytf (&F° i o
l&f0 /6?~6 1 O
/£f£ (701- '' 0
I?02. irofr ; O
13 i IJO& ' 17/V \ O
14 L?/_£ ^J??0 • 0
15 i /?io p?c o
16 }7^& '// '// £9
17 ! :
18 !
19
20
Average
0
o
O
o "••
o 	
0
o
0 	 _ j
&
£)
0
(^
•• o
o
o
o
Set Number
' 21
22
23
24
25
26
27
28
29
30
31
32
33
34
35.
36
r
Start
• •!


me Opacity
End Sum Average






r
•
j






i 37 !

1 J
I
1
1









•—







•
i
! !


1

1

: 38 i i
39 !
40
i



















-------
                              Summary of Vi:,
                                                                .„.-
                                                                  *
Date:
Type of
Type of Discharge:
Location of Discharge:,
Height of Point of Discharge:
Description of Background:
Description of Sky:
Wind Direction:
Color of Plume:
Duration of Observation:
              SUMMARY OF AVERAGE OPACITY
                                             Distance  from  Observer  to Discharge Point:
                                             Height, of Observation .Pxnnt:^^**^^^^
                                             Direction of Observer from  Discharge Point: it-
                                             Wind Velocity:  'y-^/Z
                                             Detached Plume:  •  .
                                                            SUMMARY  OF AVERAGE  OPACITY
Time Opacity Time
Set- Number Start End Sum Average Set Number Start End
;. ! ,*** /O;H 0 % • 21 "
2 /0'/V it'lo
3 /o '2.0 10* iff
4 /tf'2-6 /0JJ2"
5 /D'll lo'W
6 lo'tf /0'(f
•g J0/56 H''^
• 10 il'C^ jl'6%
11 //'<55' H'Hf
' 1 2 // //^ " '2^>
13 n'.io ii'iif
. 14 iczu i''r~
15 //;-32. /''-3S-
16 //'•*£ //'vy
/ 22
23
24 •
25
26
27
28
29 '
30
31
32
33
34
35
A 36
17 //'-^y //•
-------
Su;;.;;;ury of Vi   i;"ic
Type uf Plant: //-'


Type of Discharge:


Location of Discharge:/?^-1"'''^' ST't-(-


Height of Point of Discharge: "^ 3&


Description of Background:  Pttsf £/ry


Description of Sky:
                     ;

Wind Direction:    /l/£


Color of Plume:  A/^y


Duration of Observation: loog-//Vff


              SUMMARY  OF  AVERAGE  OPACITY
                                                             x
               Distance from Observer to Discharge Point:


               Height of Observation Point: (5-AO  Lt^-L.


               Direction of Observer from Discharge Point:  £
               Wind Velocity:  8 -


               Detached Plume:  ^o~r
                              SUMMARY OF AVERAGE OPACITY
Time
Opacity . • T
.Set Number Start End Sum_
. 1
...
3
" 4 r_i"
6 	
•7
8 •
•9
10
11
12
>/V 02
102-0 {0z
012, /07
tO}# (0 4
JoJ/y (M
(o ro {0$
lo M /(A
J/V2- JL&
///iff ///
///
-------
uoio:
     of
A&&^S
Type of Discharge:
Location of Discharge:
Height of Point of  Discharge:^3<2
Description of Background:
Description of Sky:
Wind Direction:
Color of Plume:
Duration of Observation:
              SUMMARY OF AVERAGE  OPACITY
Distance from Observer  to  Discharge Point:~
Height, of Observation Point: jA&^v1 x«*~
Direction of Observer'from Discharge Point:
              Wind  Velocity: <£-
              Detached Plume:
                             SUMMARY OF AVERAGE OPACITY
Time • • Opacity Time Opacity
Set Number Start End Sum Average Set Number Start End Sum Average
.,- • f) O ' " — '/- t£"-?r> (0 0
1 /3-'fy \3:2e Q
2 fi'io /3'iff
3 >$'2'£ /3'3z-
4 /3'$2 '3-3?
5 /3'-3fr- n'H5'5~£ /v'<32-
•g m'.o'L- m'stfr
10 W'6% /•/'//
n /£/ '/K /v ' 22'
19 /^;<9^ /5'<5>^
20 l^'Oy ^''ly \

















; ^
21 'o-7/ __
22 * 'ic'" ?i_
23 r'5"''2^ "°
24
?^ *GR£fiK\
C-^ — ^
26
27 u^;j<9 /i"rr<>
28 /5~:5^ '£;p2-
29 /fr7tf^' x^?^
30 /6^S" Ik'iV
31 /t.7/y /^x2^
32 /t;2o ^'^^
33 ;6«'?^ /£'?2
34 . /^?3Z '/frHJ'
**s ^ ^ ^ .^ . . ^" j ^ /y
35 y^'3^ lU'W
36 /fr^-ff tb'')&
37 /^^^? Ik's Si*
38 * Avf5^ /7'^ ^
39 ?££rf^ f
40 ^y?-"^ x?'/v
••-• 	 - 	 - . . ^/ /7{^ /77''?1/
V3 i?;^ i7' 3^
i T
W_ 17.^ /?rsr
/7 ^7'Vy /7'5"0






















•
. i



















—



/

-------
                          Sui;.;;;<3ry of V"1 ale Dnis.sious
Date:  /

Type- uf Plant:  ASPHALT.

Type of Discharge:   STAC/T

Location of Discharge:/^^-^''^^ 3V/££
                                         Distance from Observer to Discharge Point:

                                         Height of Observation Point:
                                     F
Height of Point of Discharge:

Description of Background: /t

Description of Sky:

Wind Direction:

Color of Plume:

Duration of Observation:

              SUKMARY OF AVERAGE OPACITY
                                       US///-T£
                                          Direction of Observer from Discharge J'oi/it:
                                                                          sC?  * p^ C-

                                                      , <>*#*'
                                          Wind  Velocity:

                                          Detached  Plume:
                                                         SUW-1ARY OF AVERAGE  OPACITY
               Time
                               Opacity
                                                                Time
                                                                              Opacity
,Set  Number   Start    End
                                 Average   Set Number     Start
                                                                 End
                                                                           Sum
                                                                                  Average
   _]
    2"
    3
    4
    5
    6
   _7_
    8
_?
 IP
 LL
 12.
 13
                I
                                 0
                                 o
                           !.  Y. .

                           \  O
                                                 2.1
                                                 22
                                                 23
                                                _24_
                                                 25
         7/7*
                                    P.
                                    0
                             0"
                                    ..Q-
                                                 26
                                                 27
                                                 28
                                                ~29
                                                 30"
                                                       /rr7
                                                                        o
                                                                                   O
                                                                                   0
                                                                                   o
                                                                                  ~o
                                                                        0
                                                                           -Q—r
                                                          0) J l(,0c(  	Q_
                                                             "  \/G/f~\   O
                                                                           -+
                                                                               o
                                 0
                                                31
                                                              i /62. 7 \    n
                                 n
                                                 32
                                                             ~?J
                          0
                                    o
                                                 33
                                                                                   o
H
15
                 xv/^
                                     n
                                                 34
                                                                             o
                          0
                                     0
                                                 35
                                                                   7^7     fr
1 6
                             0
                                     o
                                                 35
                                                                          o
1L
is.
T9_
20
                          0
                                     0
                                                 37
                          (7
                                    0
                                                 38
                                                                            O
                          0
                                     ft
                                                 39
                                                                             n
                                 0
                                                 40
                                                                   17 ?S
                                                       /7>
                                             VJ

                                             vy
                                                                            O
                                                                            O
                                                                            o

                                                                            o
                                                                                o

-------