United States
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park NC 27711
EMB Report 79-MET-4
January 1980
Air
Metallic Minerals
Emission Test Report
Cyprus Bagdad Copper
Company
Bagdad, Arizona
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FINAL REPORT
2701-01-0280
Emission Test Report
Cyprus Bagdad Copper Mine
Bagdad, Arizona
EMB Report No. 79-MET 4
EPA Contract No. 68-02-2813
Work Assignment No. 43
Prepared For
Environmental Protection Agency
Emission Measurement Branch
ESED, Mail Drop #13
Research Triangle Park, N. C. 27711
February 14, 1980
by
SCOn ENVIRONMENTAL TECHNOLOGY, INC.
2600 Cajon Boulevard
San Bernardino, California 92411
Scott Environmental Technology Inc.
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TABLE OF CONTENTS
Page Number
LIST OF FIGURES — — — - 1
LIST OF TABLES - ^ - 11
1.0 INTRODUCTION —— - 1
2.0 PR'OCESS DESCRIPTION - 6
2\\ PRIMARY CRUSHER —— 7
2.2 SECONDARY CRUSHER AND RECLAIMED ORE 7
2.3 TRUCK LOADOUT - -— 7
2.4 PRIMARY CRUSHER - TRUCK UNLOADING - — 7
2.5 SECONDARY CRUSHER - RECLAIM AREA — - 8
2.6 TRUCK LOADOUT- 10
3.0 SUMMARY AND DISCUSSION OF RESULTS — 12
3.1 PRIMARY CRUSHER — — - — 12
3.2 SECONDARY CRUSHER 15
3.3 TRUCK LOADOUT- - - -— — 39
3.4 TRACE ELEMENT ANALYSIS —— 39
4.0 SAMPLING AND ANALYTICAL PROCEDURES 89
4.1 EPA METHOD #1 - SELECTION OF SAMPLING LOCATION- — 89
4.2 EPA METHOD #2 - MEASUREMENT OF GAS VOLUME FLOW RATE 89
4.3 DETERMINATION OF MOISTURE CONTENT OF STACK GASES-— 90
4.4 DETERMINATION OF PARTICULATE EMISSIONS — — 90
4.5 DETERMINATION OF VISIBLE EMISSIONS — - 90
4.6 DETERMINATION OF PARTICLE SIZE —— 90
APPENDIX A - COMPLETE PARTICULATE RESULTS INCLUDING FORMULAE USED
IN THE CALCULATIONS - A-l
APPENDIX B - PARTICULATE FIELD DATA SHEETS B-l
APPENDIX C - PARTICLE SIZE FIELD DATA SHEETS C-l
APPENDIX D - VISIBLE EMISSIONS FIELD DATA SHEETS - - - D-l
APPENDIX E - EQUIPMENT CALIBRATIONS AND SMOKE READER CERTIFICATIONS— E-l
APPENDIX F - TRACE ELEMENT ANALYSIS F-l
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LIST OF FIGURES
Page Number
Figure 1 - Schematic Diagram of Primary Crusher 3
Figure 2 - Schematic Diagram of Secondary Crusher and Ore Reclaim 4
Figure 3 - Schematic Diagram of Truck Loadout 5
Figure 4 - Primary Crusher Conveyor, Runs 1, 2 and 3 26
Figure 5 - Primary Crusher Surge Bin, Runs 1, 2 "and 3 27
Figure 6 - Primary Crusher Scrubber Inlet, Runs 1, 2 and 3 28
Figure 7 - Primary Crusher Scrubber Outlet, Run 1 29
Figure 8 - Secondary Crusher Exhaust, Runs 4, 5 and 6 47
Figure 9 - Secondary Crusher Scrubber Inlet, Runs 4, 5 and 6 48
Figure 10- Secondary Crusher Scrubber Outlet, Run 6 49
Figure 11- Truck Loadout Conveyor Exhaust, Runs 7 and 8 72
Figure 12- Truck Loadout Exhaust Hood, Runs 7 and 8 73
Figure 13- Particulate Sampling Train 91
Figure 14- Particle Size Distribution Sampling Train 92
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LIST OF TABLES
Page Number
Table 1 - Sampling Location 2
Table 2 - Summary of Particulate Results-Primary Crusher Conveyor
Exhaust 12
Table 3 - Summary of Particulate Results-Primary Crusher Surge
Bin Exhaust 13
Table 4 - Summary of Particulate Results-Primary Crusher Scrubber
Inlet 13
Table 5 - Summary of Particulate Results-Primary Crusher Scrubber
Outlet 14
Table 6 - Summary of Control Efficiency-Primary Crusher Scrubber 14
Table 7 - Particle Size Distribution Analysis-Primary Crusher
Conveyor, Run 1 • 16
Table 8 - Particle Size Distribution Analysis-Primary Crusher
Conveyor, Run 2 17
Table 9 - Particle Size Distribution Analysis-Primary Crusher
Conveyor, Run 3 18
Table 10 - Particle Size Distribution Analysis-Primary Crusher Surge
Bin, Run 1 : 19
Table 11 - Particle Size Distribution Analysis-Primary Crusher Surge
Bin, Run 2 — - — 20 .
Table 12 - Particle Size Distribution Analysis-Primary Crusher Surge
Bin, Run 3 21
Table 13 - Particle Size Distribution Analysis-Primary Crusher
Scrubber Inlet, Run 1 22
Table 14 - Particle Size Distribution Analysis-Primary Crusher
Scrubber Inlet, Run 2 23
Table 15'- Particle Size Distribution Analysis-Primary Crusher
Scrubber Inlet, Run 3 -- 24
Table 16 - Particle Size Distribution Analysis-Primary Crusher
Scrubber Outlet, Run 1 25
Table 17 - Summary of Results of Opacity Readings-Primary Crusher
Conveyor Transfer Point, Run 1 30
Table 18 -'Summary of Results of Opacity Readings-Primary Crusher
Conveyor Transfer Point, Run 2 31
Table 19 - Summary of Results of Opacity Readings-Primary Crusher
Conveyor Transfer Point, Run 3 32
Table 20 - Summary of Fugitive Emissions-Primary Crusher Conveyor
Transfer Point, Runs 1, 2 and 3 -- 33
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LIST OF TABLES - continued
Page Number
Table 21 - Summary of Results of Opacity Readings-Primary Crusher
Scrubber Outlet, Run 1 34
Table 22 - Summary of Results of Opacity Readings-Primary Crusher
Scrubber Outlet, Run 2 35
Table 23 - Summary of Results of Opacity Readings-Primary Crusher
' Scrubber Outlet, Run 3 - 36
Table 24 - Summary of Particulate Results-Secondary Crusher Exhaust,
Runs 4, 5 and 6 - 37
Table 25 - Summary of Particulate Results-Secondary Crusher Scrubber
Inlet, Runs 4, 5 and 6 37
Table 26 - Summary of Particulate Results-Secondary Crusher Scrubber
Outlet, Runs 4, 5 and 6 - 38
Table 27 - Summary of Control Efficiency-Secondary Crusher Scrubber,
Runs 1, 2 and 3 38
Table 28 - Particle Size Distribution Analysis-Secondary Crusher
Exhaust, Run 4 40
Table 29 - Particle Size Distribution Analysis-Secondary Crusher
Exhaust, Run 5 41
Table 30 - Particle Size Distribution Analysis-Secondary Crusher
Exhaust, Run 6 - — 42
Table 31 - Particle Size Distribution Analysis-Secondary Crusher
Scrubber Inlet, Run .4 '• 43
Table 32 - Particle Size Distribution Analysis-Secondary Crusher
Scrubber Inlet, Run 5 44
Table 33 - Particle Size Distribution Analysis-Secondary Crusher
Scrubber Inlet, Run 6 45
Table 34 - Particle Size Distribution Analysis-Secondary Crusher
Scrubber Outlet, Run 6— 46.
Table 35 - Summary of Results of Opacity Readings-Secondary Crusher
Tunnel Outlet, Run 4 50'
Table 36 - Summary of Results of Opacity Readings-Secondary Crusher
Tunnel Outlet, Run 5 51
Table 37 - Summary of Results of Opacity Readings-Secondary Crusher
Tunnel Outlet, Run 6 52
Table 38 - Summary of Fugitive Emissions-Secondary Crusher Tunnel
Outlet, Runs 4, 5 and 6 - 53
Table 39 - Summary of Results of Opacity Readings-Secondary Crusher
Reclaim Feeder Hood, Run 4 54
Table 40 - Summary of Results of Opacity Readings-Secondary Crusher
Feeder Hood, Run 5 55
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LIST OF TABLES - continued
Page Number
Table 41 - Summary of Results of Opacity Readings-Secondary Crusher
Feeder Hood, Run 6 56
Table 42 - Summary of Fugitive Emissions-Secondary Crusher Feeder
Hood, Runs 4, 5 and 6 57
Table 43 - Summary of Results of Opacity Readings-Secondary Crusher ;
Exhaust, Run 4 58
Table 44 - Summary of Results of Opacity Readings-Secondary Crusher
Exhaust, Run 5 59
Table 45 - Summary of Results of Opacity Readings-Secondary Crusher
Exhaust, Run 6 60
Table 46 - Summary of Fugitive Emissions-Secondary Crusher Exhaust,
Runs 4, 5 and 6 61
Table 47 - Summary of Results of Opacity Readings-Secondary Crusher
Baghouse Outlet, Run 4 62
Table 48 - Summary of Results of Opacity Readings-Secondary Crusher
Baghouse Outlet, Run 5 63
Table 49 - Summary of Results of Opacity Readings-Secondary Crusher
Baghouse Outlet, Run 6 64
Table 50 - Summary of Particulate Results-Truck Loadout Conveyor
Exhaust, Runs 7, 8 and 9 65
Table 51 - Summary of Particulate Results-Truck Loadout Hood Exhaust,
Runs 7, 8 and 9 66
Table 52 - Summary of Particulate Results-Truck Loadout Baghouse
Outlet, Runs 7, 8 and 9 66
Table 53 - Summary of Control Efficiency-Truck Loadout Baghouse,
Runs 1, 2 and 3 67
Table 54 - Particle Size Distribution Analysis-Truck Loadout Conveyor
Exhaust, Run 7 68
Table 55 - Particle Size Distribution Analysis-Truck Loadout Conveyor
Exhaust, Run 8 69
Table 56 - Particle Size Distribution Analysis-Truck Loadout Exhaust
Hood, Run 7 - 70
Table 57 - Particle Size Distribution Analysis-Truck Loadout Exhaust
Hood, Run 8 71
Table 58 - Summary of Results of Opacity Readings-Truck Loadout Hood,
Run 7 74
Table 59 - Summary of Results of Opacity Readings-Truck Loadout Hood,
Run 8— 75
Table 60 - Summary of Results of Opacity Readirgs-Truck Loadout Hood,
Run 9- 76
Table 61 - Summary of Fugitive Emissions-Truck Loadout Hood, Runs
7, 8 and 9 - - 77
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LIST OF TABLES - continued
Page Number
Table 62 - Summary of Results of Opacity Readings-Truck Loadout
Conveyor Hood, Run 7 78
Table 63 - Summary of Results of Opacity Readings-Truck Loadout
Conveyor Hood, Run 8 79
Table 64 - Summary of Results of Opacity Readings-Truck Loadout
I Conveyor Hood, Run 9 80
Table 65 - Summary of Results of Opacity Readings-Railroad Car Loading
: Chute, Run 7— 81
Table 66 - Summary of Results of Opacity Readings-Railroad Car Loading
Chute, Run 8- — - — - 82
Table 67 - Summary of Results of Opacity Readings-Railroad Car Loading
Chute, Run 9 -- — - 83
Table 68 - Summary of Fugitive Emissions-Railroad Car Loading Chute,
Runs 7, 8 and 9 - 84
Table 69 - Summary of Results of Opacity Readings-Truck Loadout Baghouse
Outlet, Run 7 85
Table 70 - Summary of Results of Opacity Readings-Truck Loadout Baghouse
Outlet, Run 8 - 86
Table 71 - Summary of Results of Opacity Readings-Truck Loadout Baghouse
Outlet, Run 9 87
Table 72 - Weight of Ore Concentrate Unloaded By Trucks During Test
Periods - — - 88
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1.0 INTRODUCTION
Testing to determine emissions from three operations involved in
the processing of copper ore at the Cyprus Bagdad Copper Mine in Bagdad,
Arizona for the Emissions Measurement Branch of the United States Environ-
mental protection Agency under Contract No. 68-02-2813, Work Assignment
No. 43. Testing was conducted from November 13 to November 17, 1979.
The three processes evaluated were the primary ore crushing, ore
reclaim and secondary crushing, and ore concentrate truck loadout. The
testing involved determining particulate concentration, gas flow rates, and
particle size distributions upstream and downstream from air pollution control
equipment. Visible emissions using EPA Method #9 (smoke density) and
Method #22 (duration of fugitive emissions) were also evaluated at various
points in the system. Table 1 lists the sampling locations. Figures 1,
2 and 3 show schematic diagrams of the processes and the sampling locations,
Test arrangements were made through Mr. Gene Hedden, Safety Director,
Mr. Ken Apland, Concentration Manager and Mr. Roger Wakefield, all of the
Cyprus Bagdad Copper Company. Mr. Dennis Holzschuh of the Environmental
Protection Agency was present during the tests, as was Mr. Tanhum Goldschmid
of GCA Corporation, who monitored the plant process during the tests. Scott
personnel were Messrs. Jim Reese, Joe Wilson, Maynard Johnson, Am Cipollone,
Tim Sharp, Bernie Roth, Dave Combe, Tony Guastella, Joe Marino, Bruce Markley,
Steve Fisher and Tom MacNeel.
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a]
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Process
Primary Crusher
TABLE 1
SAMPLING LOCATION
Location
Conveyor Exhaust
Surge Bin Exhaust
Scrubber Inlet
Scrubber Outlet
Tests Conducted
EPA Methods 5, 9, and 22, and particle size
EPA Method #5 and particle size
EPA Method #5 and particle size
EPA Methods #5 and #9, and particle size
=*=
PO
I
CD
H-*
I
O
ro
oo
o
Secondary Crusher
Tunnel Outlet
Feeder Hood
Crusher Exhaust
Scrubber Inlet
Scrubber Outlet
EPA Methods #9 and #22
EPA Methods #9 and #22
EPA Methods #5, #9 and #22, and particle size
EPA Method #5 and particle size
EPA Methods #5 and #9, and particle size
Truck Loadout
Railroad Car Loading Chute
Conveyor Exhaust
Loadout Hood Exhaust
Baghouse Outlet
EPA Methods #9 and #22
EPA Methods #5, #9, #22 and particle size
EPA Method #5 and particle size
EPA Methods #9 and #22
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Scrubber
To Mill
Storage Pile
To Atmosphere
A
Scrubber Outlet
Sampling Location
Conveyor Exhaust
Sampl ing^Location
.Scrubber Inlet
Sampling Location
Surge Bin Exhaust
Sampling Location
Conveyor No.
V/\/\/v\ Ground Level
f V Primary Crusher
Surge Bin
Conveyor No. 1
=«=
IV)
-~J
o
i—*
i
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I—>
I
o
no
oo
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CO
FIGURE 1 - SCHEMATIC DIAGRAM OF PRIMARY CRUSHER
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To Atmosphere
Scrubber Outlet Sampling Locftti'on
Scrubber
Scrubber Inlet
Sampling Location
Crusher Exhaust
Sampling Location
Secondary
Crusher
Crusher Exhaust
Visible
Emissions Test
Location
Conveyor to Mill
FIGURE 2 - SCHEMATIC DIAGRAM OF SrCONDARY CRUSHER AND
ORE RECLAIM
ro
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CO
o
Tunnel
Outlet Test
Location
Feeder Hood
Test Location
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Scrubber Outlet
Sampling Location
To
Atmosphere
Railroad Car Loading Chute
and Test Location
Loadout Hood
Sampling Location
Truck Loadout Hood
Conveyor
Exhaust
Sampling
Location
Loadout Hood Visible
Emissions Test Location
Conveyor Exhaust Visible '
Emissions Test Location
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FIGURE 3 - SCHEMATIC DIAGRAM OF TRUCK LOADOUT
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2701-01-0280 -6-
2.0 PROCESS DESCRIPTION
The Cyprus Bagdad copper mill was completed in mid-1977 with a
capacity of 36,000 metric tons (MT) (40,000 tons)/day and is operated 24
hours/day. Copper and molybdenum are recovered from quartz-monzonite rock
with average contents of .49% copper, .03% copper oxide, and .03% MoS?.
Ore is loaded at the pit into 150 MT (170 ton) trucks and moved
to the west end of the pit where the primary crusher is located. The primary
crusher is a 152 x 226 cm (60 x 89 inch) Allis Chalmers gyratory with an
hourly capacity of 3,266 MT (3,600 tons). Ore is reduced to <23 cm (9 inches).
The trucks usually unload every 2 to 3 minutes and the corresponding crushing
cycle lasts a similar time period. Ore is then conveyed and elevated,
respectively, 1,950 meters (6,400 feet), and 310 meters (1,020 feet). The
crushed ore passes 4 transfer points to radial stackers that feed a 50,000 MT
(55,000 ton) live ore storage and 140,000 MT (150,000 ton) dead ore storage.
Ore is continually reclaimed by a conveying system under the stock-
pile into the feed' hopper for the wet grinding. Ore enters 1 of 3 parallel
autogenous (wet) mill lines at an approximate hourly rate of 550 MT (600 tons)
per line. After milling, material is screened with processed ore >3.8 cm
(1.5 inch) being sent to a Symons secondary (2.1 m [7 ft.]) shorthead crusher
and returned with the reclaimed ore to the mill process.
After milling, processed ore is floated and cleaned with a
thickener, dewatered by drum filters, and dried by a parallel flow dryer.
Copper concentrate is then transferred by belt conveyors to an enclosed stock-
pile, and frontend loaded into 23 MT (25 ton) covered trucks. An average daily
rate of 30-35 trucks transport concentrate 34 Km (21 miles) to. a railhead that
fills railcars which are conveyed to a Phelps-Dodge smelter at Hidalgo, New
Mexico.
Molybdenum is floated and cleaned in a copper-molybdenum thickener,
with underflow dewatered by a drum filter, and dried in a hoi oflite dryer.
The end product is 90% Mo$2 and is packed in drums and shipped overseas.
A detailed description of the control equipment that was tested is
given in the following sections.
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2.1 PRIMARY CRUSHER
Ore is received in a cyclic nature as mentioned above. Emissions
are picked up at the primary cursher surge bin and from two conveyor transfer
points. A diagram is shown in Figure 1 (Page 3). Wet suppression is applied
p
using NALCO 8800 surfactant and water to both sides of the crusher pit, at
the apron feeder to Conveyor No. 1 and at the transfer point between Conveyors
No. 1 and No. 2. Operating parameters for the .American Air Filter Rotoclone
supplied by the plant are 270m3/min (9,500 scfm), 22°C (71°F), inlet concen-
3 3
trations of .44 g/m (.193 gm/dscf) and outlet concentration of .01 g/m
(.005 gm/dscf).
2.2 SECONDARY CRUSHER AND RECLAIMED ORE
The autogenous (wet) mill is continually fed ore from the reclaim
area. Emissions are picked up from the feeder hoods as ore is transferred
from the storage area to be conveyed to the wet mill and from the Symons 7-foot
shorthead crusher which crushes ore >l-l/2 inch leaving the mill. A diagram is
shown in Figure 2 (Page 4). Operating parameters for the Ducon UW-4, Model III
wet scrubber supplied by the plant are 410 m /mi.n. (14,400 scfm), 18°C (64°F),
•3
inlet concentration of 1.6 g/m (.68 gr/dscf) and outlet concentration of
.001 g/m3 (.0006 gr/dscf).
2.3 TRUCK LOADOUT
Ore is received in a cyclic nature as mentioned above. Emissions are
picked up from the loadout pit and from the transfer point from the pit to the
railcar loading conveyor. A diagram is shown in Figure 3 (Page 5). Operating
parameters for the Fabric-Jet baghouse are 88 m /min. (3,100 scfm) and ambient
temperatures.
2.4 PRIMARY CRUSHER - TRUCK UNLOADING
Emission tests were run on November 13, 1979 and processes operated
smoothly except for a 3-hour period when crushing was stopped so that the mill
could process some of the excess in the crushed ore storage pile. The average
hourly rate in August 1979 was 2,750 MT (3,030 tons). During testing, the
following production rates were read from a gauge in the control room:
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Time
10:00 AM
10:30 AM
5:30 PM
6:30 PM
7:30 PM
8:30 PM
9:30 PM
10:30 PM
11:00 PM
MT/Hr
2050*
1487
2730
2750
3290
2730
2750
2740
1770*
* Half-hour rate
A summary of Methods 9 and 22 observations follows:
Method 9
Location
Primary Crusher Conveyor
Transfer Point
Scrubber Outlet
Date
No. of 6 Min.
Intervals
Opacity Reading (%)
(6 Min. Average)
Average Maximum
11-13-79
11-13-79
11-13-79
11-13-79
11-13-79
11-13-79
10
8
8
14
13
8
15
15
10
5
5
10
20
15
15
10
10
10
Location
Primary Crusher Con-
veyor Transfer Point
Method 22
Date
Test Duration
(Seconds)
Fugitive Emissions
Seconds %
11-13-79
11-13-79
11-13-79
4102
3320
3361
4042
3274
3259
99
99
97
2.5 SECONDARY CRUSHER-RECLAIM AREA
Emission tests were run on November 14 and 15, 1979 and process was
normal except for a period when the water level in the scrubber water reservoir
fell below a critical level causing testing to be discontinued. Two gauges
located in the reclaim tunnel were read simultaneously to record amount of ore
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entering the mill and the rate of recycled ore. Thus, production rate is the
difference between these two readings. The average hourly rate in August 1979
was 530 MT (580 tons) for Line No. 1. During testing, the following readings
were recorded:
November 14, 1979
Time
2:10 PM
2:40 PM
3:10 PM
4:10 PM
5:10 PM
Recycled
(Metric Tons)
4340
4440
4540
. 4710
7650
Total
(Metric Tons)
16040
16520
16820
17550
18360
Production
Rate
(MTPH)
380
580
570
600
November 15, 1979
8:00 AM
8:30 AM
9:00 AM
10:00 AM
11:00 AM
12:00 PM
1:00 PM
2:00 PM
3:00 PM
8010
8110
8220
8400
8590
8780
8980
9180
9370
29510
29820
30230
30870
31520
32240
32980
33730
34500
520
460
450
460
800
540
550
580
A summary of Method 9 observations follows:
Location Date
Secondary Crusher Tunnel 11-14-79
Outlet
Secondary Crusher
Reclaim Feeder Hood
Secondary Crusher 11-15-79
Reclaim Feeder Hood
Second. Crusher Exhaust 11-14-79
Second. Crusher Exhaust 11-15-79
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Scott Environmental Technology Inc
No. of 6 Min.
Intervals
25 ..
11-15-79
11-15-79
11-14-79
19
20
25
35
19
31
Opacity Reading (%)
(6 Min. Average)
Average Maximum
...0
0
0
0
4
5
0
0
0
0
8
9
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#2701-01-0280
Location
-10-
Date
No. of 6 Min.
Intervals
Opacity Reading (%)
(6 Min. Average)
Average Maximum
Secondary Crusher Outlet 11/14/79
Secondary Crusher Outlet 11/15/79
17
37
0
0
0
0
Method 22
Location
Secondary Crusher
Tunnel Outlet
Secondary Crusher
Tunnel Outlet
Secondary Crusher
Feeder Hood
Secondary Crusher
Feeder Hood 11/15/79
Secondary Crusher Exhaust 11/14/79
Secondary Crusher Exhaust 11/15/79
Date
11/14/79
11/15/79
11/14/79
lest Duration
(Seconds)
9120
14400
9000
10538
6279
10790
Fugitive Emissions
Seconds %
0
0
1265
4686
9007
0
0
12
75
83
2.6 TRUCK LOADOUT
Emission tests v/ere run on November 16 and 17, 1979 during the unloading
of concentrate which is a cyclic operation. Individual truck weights were
measured at the Bagdad plant. During August 1979, the average daily concentrate
trucked was 160 MT. It takes approximately 15 minutes for trucks to offload.
During testing, the following process information was obtained:
Date
11-16-79
11-17-79
11-17-79
Truck Loadout
Times
1155-1420
800-1110
1100-1455
Number of
Trucks
7
7
6
Total Weight
(MT)
158
158
136
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A summary of Methods 9 and 22 observations follows:
Method 9
Location
Truck Loadout Hood
Truck Loadout Hood
Truck Loadout Hood
Truck Loadout Conveyor Hood
Truck Loadout Conveyor Hood
Truck Loadout Conveyor Hood
Rail car Loading Chute
Rail car Loading Chute
Railcar Loading Chute
Baghouse Outlet
Baghouse Outlet
Baghouse Outlet
Date
11-16-79
11-17-79
11-17-79
11-16-79
11-17-79
11-17-79
11-16-79
11-17-79
11-17-79
11-16-79
11-17-79
11-17-79
No. of 6 Min.
Intervals
8
7
7 -
9
8
8
7
7
9
8
7
9
Opacity
(6 Min
Average
0
0
0
15
0
0
0
5
0
0
0
0
Reading (%)
. Average)
Maximum
0
0
0
25
5
5
5
5
5
0
0
0
Method 22
Location
Truck Loadout Hood
Truck Loadout Hood
Truck Loadout Hood
Rail Car Loading Chute
Rail Car Loading Chute
Rail Car Loading Chute
Date
Test Duration
(Seconds)
Fugitive Emissions
Seconds %
11-16-79
11-17-79
11-17-79
11-16-79
11-17-79
11-17-79
4380
4020
4020
4320
3960
4080
3678
1734
1721
3429
3234
3037
84
43
43
79
82
74
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3.0 SUMMARY AND DISCUSSION OF RESULTS
3.1 PRIMARY CRUSHER
Testing for particulates was conducted in the exhaust duct from the
Conveyor 1 to Conveyor 2 transfer point (conveyor exhaust), the surge bin
exhaust duct, the scrubber inlet, and the scrubber outlet. Visible emissions
were monitored at the hood over the Conveyor 1 to Conveyor 2 transfer point
(Method #9 and Method #22) and at the scrubber outlet (Method #9). Results of
the particulate testing are summarized in Tables 2 through 5. The control
efficiency of the primary-crusher scrubber is summarized in Table 6. Complete
particulate results, including formulae used in the calculations, are included
in Appendix A. Field data sheets are included in Appendix B.
TABLE 2
SUMMARY OF PARTICULATE RESULTS
Primary Crusher Conveyor Exhaust
Date: November 13, 1979 Average
Time Started: 0923 1335 1700
Time Ended: 1033 1448 1820
Run No.: 123
Gas Flow Rate, (dscfm): 1350 1410 2590 1783
Actual Gas Flow Rate,
(acfm): 1513 1590 2930 2011
Particulate Concen-
tration (gr/dscf) 0.0585 0.0916 0.0697 0.0733
Particulate Mass Flow
Rate, (Ibs/hr) 0.68 1.1 1.5 1.09
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TABLE 3
SUMMARY OF PARTICULATE RESULTS
Primary Crusher Surge Bin Exhaust
Date: : November 13, 1979 Average
Time Started: 0915 1340 1730
Time Ended: 1020 1445 1838
Run No.: 1 2 3
Gas Flow Rate (dscfm): 1880 "1850 1820 1850
Actual Gas Flow Rate
(acfm): 2100 2120 2080 2100
Particulate Concen-
tration (gr/dscf): 0.928 0.701 0.862 0.830
Particulate Mass Flow
Rate, (Ibs/hr): 15.0 11.1 13.5 13.2
TABLE 4
SUMMARY OF PARTICULATE RESULTS
Primary Crusher Scrubber Inlet
Date: . November 13, 1979 Average
Time Started: 0915 1340 1715
Time Ended: 1030 1450 1830
Run No.: 123
Gas Flow Rate, (dscfm): 7010 6560 6570 6713
Actual Gas Flow Rate,
(acfm): 7590 7380 7430 7467
Particulate Concen-
tration, (gr/dscf): 0.105 0.316 0.236 0.219
Particulate Mass Flow
Rate, (Ibs/hr): 6.3 17.8 13.3 12.5
; Scott Environmental Technolosy Inc.
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#2701-01-0280 -14-
TABLE 5
SUMMARY OF PARTICIPATE RESULTS
Primary Crusher Scrubber Outlet
Date: November 13, 1979 Average
Time Started: 0904 1331 1630
Time Ended: 1032 1454 1816
Run No.: 12 3
Gas Flow Rate (dscfm): 7400 7080 7020 7167
Actual Gas Flow Rate,
(acfm): 8160 7920 7940 8007
Particulate Concen-
tration, (gr/dscf): 0.0109 0.0115 0.0095 0.0106
Particulate Mass Flow
Rate, (Ibs/hr): 0.68 0.69 0.57 0.65
TABLE 6
SUMMARY OF CONTROL EFFICIENCY
Primary Crusher Scrubber
Run No.: 1 2 3 Avg.
#
Control Efficiency (%}: 89.2 96.1 95.7 93.7
A duct, exhausting the one transfer point from the surge bin area to
Conveyor 1 was net sampled, but also feeds into the scrubber inlet. The gas
flow and particulate mass flow rates in this duct can be estimated by subtracting
1 Scott Environmental Technology Inc.
-------
#2701-01-0280 -15-
the flows in the conveyor exhaust and surge bin exhaust ducts from the flow in
the scrubber inlet duct.
The gas flow rate at the conveyor exhaust sampling location was
significantly higher during Run No. 3 than during Runs No. 1 and No. 2. There
is no apparent reason for this difference. The duct system has been modified
since the original installation.
The particulate concentration and corresponding mass flow rate at
the scrubber inlet sampling location was considerably lower during Run No. 1
than during Runs No. 2 and No. 3. This low concentration was the cause of the
lower collection efficiency of the scrubber for Run No. 1. This value appears
low because the sum of the particulate mass flow rates at the conveyor exhaust
and the surge bin exhaust is much higher than the mass flow rate measured at the
scrubber inlet. The agreement between the conveyor and surge bin exhausts and
the scrubber inlet is much better for Runs No. 2 and No. 3.
Results of the particle size analyses at the primary crusher are
summarized in Tables 7 through 16 and in Figures 4 through 7. The field
data sheets are included in Appendix C.
The results of visible emissions observations at the Conveyor No. 1
to Conveyor No. 2 transfer point are summarized in Tables 17 through 19
(smoke density) and Table 20 (fugitive emissions). Results of visible
emissions observations at the scrubber outlet are summarized in Tables 21
through 23. These results show the opacity averaged from 5% to 20% at the
conveyor transfer hood. The opacity averaged from 0 to 10% at the scrubber
outlet. Field data sheets are included in Appendix D.
3.2 SECONDARY CRUSHER
Testing for particulate matter at the secondary crusher and ore
reclaim process was conducted on the duct exhausting the secondary crusher,
on the scrubber inlet (which includes the secondary crusher exhaust and the
feeder hood exhausts), and the scrubber outlet. Visible emissions were monitored
at the secondary crusher exhaust hood, one of the feeder exhaust hoods, the
exit from the tunnel in which the conveyor serving the crusher and the ore
feeders is located, and the scrubber outlet.
; Scott Environmental TechndcKjy Inc.
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#2701-01-0280
-16-
TABLE 7
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-13-79
Time: 0430
Sampling Location: Prime Crusher Conveyor
Traverse9 Point No. Sampled: 3
RunN°': *
in. Hg):
.0
rwc, 'i p> )., '{
g? S JSSA" j:
Moisture
27.06
67
20
19.68
1.0
i iu i 3 uu I c \fo [i^u;. J. • "
Meter Temperature ( F): 90.0
Flow Setting, AH" (in. O): 2-50
Nozzle Diameter (In.): -250
Sample Flow Rate (at stack conditions) - .99 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
79. 802
23.80
10.00
5.90
6.00
3.30
.40
.10
%
61.71
18.40
7.73
4.56
4.64
2.55
.30
.07
Cumulative
%
100.00
38.28
19.87
12.14
7.57
2.93
.38
.07
Back-up
Filter
.00
.00
.00
ECD1
(Micrometers)
9.82 and larger
6.26
4.12
2.85
1.82
.92
.55
.37
< 0.37
Total 129.30
1
ECD - Effective Cutoff Diameter of preceding plate.
y
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
' Scott Environmental Technology Inc.
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#2701-01-0280 -17-
TABLE 8
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-13-79 Ph^(1n- H9): 27.08
Time: 0703 bar 0
Sampling Location: Primary Crusher Conveyor^tack Tf:1p' }J.'l 6®'°
Traverse Point No. Sampled: 3 Cample Time^Min)^ 15^
Kun N0<: ^ Moisture (% FLO): 1.1
Meter Temperature ( F): 82.0
Flow Setting, AH'(in. O): 1.30
•Nozzle Diameter (In.): -250
Sample Flow Rate (at stack conditions) - .66 cfm
ECD1
(Micrometers)
12.20 and larger
7.72
5.10
3.53
2.25
1.15
.70
.47
Back-up
Filter -70 l-76 l-76 <-47
Total 39.70
ECD - Effective Cuto*ff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
27. 102
1.90
3.70
2.10
1.70
1.30
.50
.70
%
68.26
4.78
9.31
5.28
4.28
3.27
1.25
1.76
Cumulative
100.00
31.73
26.95
17.63 •
12.34
8.06
4.78 .
3.52
Scotr Environmental Technolosy Inc.
-------
#2701-01-0280 ~18-
TABLE 9
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-13-79 p (in. Hg): 27.08
Time- 1°00
Sampiing Location: Primary Crusher Conveyofack Temp. ( F): 68.0
Traverse Point No. Sampled: 3 gjple T^jHin): 20^
Run NO': ^ Moisture (55 HO): 1.1
Meter Temperature ( F): 97.0
Flow Setting, AH- (in. H?0): 1-30
Nozzle Diameter (In.): -250
Sample Flow Rate (at stack conditions) - -72 cfm
Plate Net Wt.
No. (mg) %
I 97. 602 60.13
2 26.20 16.14
3 26.00 16.01
4 6.00 3.69
5 3.40 2.09
6 2.80 1.72
7 .20 .12
8 .10 .06
Cumulative
%
100.00
39.86
23.72
7.70
4.00
1.91
.18
.06
ECD1 ' .
(Micrometers )
11.40 and larger
7.23
4.77
3.30
2.10
1.08
.65
.44
.00 .00
Total 162.30
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technobsy Inc.
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#2701-01-0280
-19-
TABLE 10
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-13-79
Time: 0450
Sampling Location:
Traverse Point No.
Run No.: 1
Primary Crusher Surge
Sampled: 3 Bin
27.06
67.0
30
Pbar(in- Hg):
Stack Temp. (°F):
Sample Time (Min):
Sample Volume (cf)
Moisture (% O):
Meter Temperature (°F): 94-°
Flow Setting, AH (in. H?0): 1-48
Nozzle Diameter (In.): -250
22.07
2.2
Sample Flow Rate (at stack conditions) - .75 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
670. OO2
4.50
7.00
5.70
8.70
9.90
3.70
.50
.00
94.36
.63
.98
.80
1.22
1.39
.52
.07
.00
Cumulative
%
100.00
5.63
5.00
4.01 -
3.21
1.98
.59
.07
ECD1
(Micrometers)
11.21 and
•7.11
4.69
3.25
2.07
1.06
.64
.43
larger
.00
4.43
Total 710.00
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technoiosy Inc
-------
#2701-01-0280
-20-
. TABLE 11
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-13-79
Time: 0700
Sampling Location: Primary Crusher Surge
Traverse Point No. Sampled: 3 Bin
Run No.: 2
Pbar(in. Hg): 27.08
Stack Temp. (°F): 66.0
Sample Time (Min): 15
Sample Volume (cf): 11.29
Moisture (% O): Q2.2
Meter Temperature ( F): 104.0
Flow Setting, AH (in. H?0): 1-48
Nozzle Diameter (In.): d -250
.Sample Flow Rate (at stack conditions) - -76 cfn1
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(nig)
298. 902
1.00
1.10
1.00
2.00
1.90
.50
.00
.00
97.55
.32
.35
.32
.65
.62
.16
.00
.00
Cumulative
%
100.00
2.44
2.12
1.76
1.43
.78
.16
.00
ECD1
(Micrometers )
11.07 and
7.03
4.64
3.21
2.05
1.05
.63
.42
larger
.00
£.42
Total 306.40
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
I Scott Environmental Technokxjy Inc
-------
#2701-01-0280
-21-
TABLE 12
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11/13/79
Time: 2150
Sampling Location: Primary Crusher Surge
Traverse Point No. Sampled: 3 Bin
Run No.:/ 3
Pbar(in. Hg): 27.08
Stack Temp. (°F): 66.0
Sample Time (Min): 15
Sample Volume (cf): 11.05
Moisture (% H?0): 2.2
Meter Temperature ( F): 82.0
Flow Setting, AH (in. H?0):
Nozzle Diameter (In.): -250
1.48
Sample Flow Rate (at stack conditions) - .75 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
1266. OO2
3.60
4.20
3.00
4.20
4-. 30
1.10
.00
.10
98.40
.27
.32
.23
.32
.33
.08
.00
.00
Cumulative
%
100.00
1.59
1.31
.98
.75
.42
.09
.00
ECD1 '
(Micrometers )
11.19 and
.7.10
4.69
3.24
2.07
1.06
.64
.43
larger
.00
4.43
Total 1286.50
1
ECD - Effective Cutoff Diameter of preceding plate.
?
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technology Inc.
-------
#2701-1)1-0280 -22-
TABLE 13
PARTICLE SIZE DISTRIBUTION ANALYSIS -
Date: 11-13-79 p (in. Hg): 27.02
Time- 1635 bar ' 0
Sampling Location: Primary Crusher Scrubber Stack Temp. F): 67.0
Averse .Point No. Sampled: 3 Inlet Sample $^,^20^
Kun N0" Moisture (% O): 1-6
Meter Temperature ( F): 108.0
Flow Setting, AH (in. H?0): 1-80
Nozzle Diameter (In.): .196
Sample Flov/ Rate (at stack conditions) - .83 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 127.602 71.72 100.00 10.61 and larger
2 19.10 10.73 28.27 6.75
3 12.60 7.08 17.53 4.45
4 5.80 3.26 10.45 3.07
5 6.00 3.37 7.19 1.96
6 6.10 3.42 3.82 1.00
7 .70 .39 .39 .60
8 ' .00 .00 .00 .40
-°° -00 -00
Total 177.90
ECD - Effective Cutoff Diameter of preceding plate.
p
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
! Scott Environmental Technolosy Inc
-------
#2701-01-0280
-23-
TABLE 14
PARTICLE SIZE /.TRIBUTION ANALYSIS
Date: 11-13-79 Pbar^in' Hg): 26'97
Sampling Location: Primary Crusher Scrubber Stack Temp. (°F): 66.0
Traverse Point No. Sampled: 3 Inlet Sample Tj-jejMin): 15^
Run NO': 2 Moisture (% HO): Q2.2
Meter Temperature ( F): 110.0
Flow Setting, AH (in. H?0): 1-80
Nozzle Diameter (In.): -196
Sample Flow Rate (at stack conditions) - .87 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
230. 802
105.50
31.60
5.85
3.40
2,50
.60
.20
%
60.64
27.72
8.30
1.53
.89
.65
.15
.05
Back-up
Filter
.10
.02
Cumulative
100.00
39.35
11.62
3.32
1.78
.89
.23
.07
.02
ECD*
(Micrometers)
10.38 and larger
6.60
4.35
. 3.01
1.92
.98
.59
.39
<.39
Total 380.55
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott EnvironmentalTechnofosyInc
-------
#2701-01-0280 -24-
TABLE 15
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: J};13-79 phar(1n- H9^: 26'97
Time* 2145 Ddr o
Sampling Location: Primary Crusher Scrubber Stack Temp. F): 66 0
Traverse Point No. Sampled: 3 Inlet Samp e Time (Mm): 15
R ., . 3 Sample Volume (cf): 11.19
Kun N°" Moisture (% H?0): 2.2
Meter Temperature ( F): 70.0
Flow-Setting, AH (in. O): 1-80
Nozzle Diameter (In.): -196
Sample Flov/ Rate (at stack conditions) - .76 cfm
Plate Net Wt. Cumulative ECD1 '
No. (mg) __% % (Micrometers)
1 188.20* 38.76 100.00 11.12 and larger
2 90.00 18.53 61.23 7.05
3 94.20 ' 19.40 42.69 4.66
4 77.70 16.00 23.29 , 3.22
5 30.20 6.22 7.29 2.05
6 4.40 .90 1.07 1.05
7 .50 .10 .16 .63
8 .30 .06 .06 .42
Back-up .00 >00 >00 ^_42
Filter ^
Total 485.50
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
\\§)\ Scott EnvironmentalTechnotosy 'rc.
-------
#2701-01-0280
. ~25"
TABLE 16
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-12-79 Pbar^1n' Hg^: 27'15
Sampling Location: Primary Crusher Scrubber Stack Temp. (°F): 67.0
Traverse Point No. Sailed: C-5 Outlet Sample Tj-eJHjn)^ 90^
Run N°" Moisture (% H?0): 1.3
Meter Temperature ( F): 80.0
Flow Setting, AH (in. H?0): 1-80
Nozzle Diameter (In.): -185
Sample Flow Rate (at stack conditions) - .82 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 15.40* 61.11 100.00 10.69 and larger
2 .10 .39 38.88 6.79
3 .00 .00 38.49 4.48
4 1.20 4.76 38.49 • 3.10
5 2.00 7.93 33.73 1.98
6 4.30 17.06 25.79 1.01
7 1.80 7.14 8.73 .61
g .30 1.19 1.58 .41
Back-up 1Q >3g -3g ^Al
Filter ^
Total 25.20
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scorr Environmental Techndosy 'nc
-------
0.01
FIGURE 4
PRIMARY CRUSHER CONVEYOR
RUN 10
RUN 2B
RUN 3 A A
Cumulative %, Less Than Stated
Particle Size
TTFTFiiTrrni
rnTiinTiiiiniiiiiiiiii
O'J '.IT
-------
0.01
K.. i .y; . l.i. fMIIL.' !•>.!••
'"VuZ KUUFrc;. r» F.SHCIC
FIGURE 5
PRIMARY CRUSHER SURGE BIN
RUN 2 Q
RUN 3 A ,_A
'I I
Cumulative %, Less Than Stated
Particle Size
-------
10JL
99.99
0.01
t .•;.-.! |.-i 1.1 1.1 ;-M'
- I T! i N'l !! ln:i
i.-T----p.yrun m.L
U UJlill
n
FIGURE 6
PRIMARY CRUSHER SCRUBBER INLET
RUN 2g
RUN 3 A A
tiii.i iiiiiini:
Cumulative %, Less Than Stated
Particle Size
TTTiTiTiTrriTimTrrrrnTiTmmirii
if) ?ti '10 -10 Hi CO
tl . i L! LJ i
-------
Ihfte
r.n co.
2 CYCLES
Ift.r. 99-99
99.9 99.8
0.01
FIGURE 7
PRIMARY CRUSHER SCRUBBER OUTLET
RUN 1
Cumulative %, Less Than Stated
Particle Size
-------
#2701-01-0280
-30-
TABLE 17
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Primary Crusher Conveyor Transfer Stack Height: 5 ft.
Test Run No.: 1 P°1nt Distance to Stack: 15 ft.
Date: 11-13-79
Color of Plume: White
Wind Direction: N/A
Sky Description:
Indoors.
Speed:
Set
Number
1
2
3
4
5
6
7
8
9
10
Overall
Time
Start End
0915
0921
0927
0933
0939
0945
1002
1008
1014
1020
Average
0921
0927
0933
0939
0945
0951
1008
1014
1020
1026
- 15
Sum
405
490
435
420
415
340
285
335
295
260
Opacity
Average
15
20
20
20
15
15
10
15
10
10
Set Time Opacity
Number Start End Sum Avcraoe
Scott Environment*' Technofogy Inc
-------
#2701-01-0280
-31-
TABLE 18
SUMMARY OF RESULTS'OF OPACITY READINGS
Location: Primary Crusher Conveyor Transfer stack Height: 5 ft.
Point
Test Run No.: 2 Distance to Stack:
Date: 11-13-79
Color of Plume: White
15 ft.
Wind Direction: N/A Speed:
Sky Description: Indoors
Set Time . Opacity
Number Start End Sum Average
.1 1330 1336 290 10
2 1336 1342 375 15
3 1342 1348 295 10
4 1348 1354 255 10
5 1414 1420 330 15
6 1420 1426 305 15
7 1426 1432 300 15
8 1432 1438 305 15
Overall Average - 15
Set Time Opacity
Number Start End Sum Averaoe
Scott Environmental Technology Inc.
-------
#2701-01-0280
-32-
TABLE 19
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Primary Crusher Conveyor Transfer stack Height: 5 ft.
Test Run No.: 3 Distance to Stack: 15 ft.
Date: 11-13-79
Color of Plume:
White
Set Time . Opacity
Number Start End Sum Average
1 " 1700 1706 310 15
2 1711 1718 335 15
3 1718 1724 245 10
4 1724 1730 215 10
5 1740 1746 275 10
6 1746 1752 170 5
7 1758 1804 170 5
8 1804 1810 190 10
Overall Average - 10
Set Time
Number Start End
Wind Direction: N/A Speed:
Sky Description: Indoors
Opacity
Sum Averaae
I Scott Environmental Technobsy Inc
-------
#2701-01-0280 _33-
TABLE 20
SUMMARY OF FUGITIVE EMISSIONS
Date: 11-13-79
Location: Primary Crusher Conveyor Transfer Point
Run No.: • 1 2 3
Time" Started: 0915 1330 1700
Time Ended: 1030 1442 1817
Test Duration (seconds): 4102 3320 3361
Cumulative Duration of
Emissions (seconds): 4042 3274 3259
Percentage of Test Duration with , „_ „,
Emissions (%): 98-5^ 98-6% 97'0%
Average (Percent): 98.0%
Scott Environmental Technology Inc.
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#2701-01-0280
-34-
TABLE 21
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Primary Crusher Scrubber Outlet
Test Run No.: 1
Date: 11-13-79
Color of Plume:
Stack Height: 30 ft.
Distance to Stack: 100 ft.
Wind Direction: SW Speed: 0-5
Sky Description: • Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Overall
Time
Start
0913
0919
0925
0931
0937
0943
0949
0955
1001
1007
1013
1019
1025
1031
Average
End
0919
0925
0931
0937
0943
0949
09.55
1001
1007
1013
1019
1025
1031
1037
- 5
Sum
185
135
145
185
160
115
105
175
135
120
110
195
175
25
Opacity
Average
10
5
5
10
5
5
5
5
5
5
5
10
5
0
Set Time Opacity
Number Start End Sum Averaae
' Scon Environmental Technology Inc
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#2701-01-0280
-35-
TABLE 22
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Primary Crusher Scrubber Outlet
Test Run No.: 2
Date: 11-13-79
Color of Plume: White
Stack Height: 30 ft.
Distance to Stack:. 100 ft.
Wind Direction: South Speed: 0-5
Sky Description: Clear
Set
Number
1 -
2
3
4
5
6
7
8
9
10
11
12
13
Overall
Time
Start
1340
1346
1352
1358
1404
1410
1416
1422
1428
1434
1440
1446
1452
Average
End
1346
1352
1358
1404
1410
1416
1422
1428
1434
1440
1446
1452
1458
- 5
Sum
120
125
150
130
155
135
135
90
240
220
165
185
170
Opacity
Average
5
5
5
5
5
5
5
5
10
10
5
10
5
Set Time Opacity
Number Start End Sum Averaae
j{\)' Scott Environmental Technology Inc.
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#2701-01-0280
-36-
TABLE 23
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Primary Crusher Scrubber Outlet
Test Run No.: 3
Date: /11-13-79
Color of Plume: White
Stack Height: 30 ft.
Distance to Stack: 100 ft.
Wind Direction: South Speed:
Sky Description: Clear
0-5
Set Time
Number Start End
1 1640 1646
2 1646 1652
3 1652 1658
4 1658 1704
5 1704 1710
6 1710 1716
7 1716 1722
8 1722 1728
Overall Average - 10
Opac i ty
Sum Average
220 10
220 10
190 10
105 5
85 5
140 5
235 10
160 5
Set Time Opacity
Number Start End Sum Averacie
-
' Scott Environmental Technokxjy Inc.
-------
#2701-01-0280 ~37~ ,
Results of the participate testing are summarized-in Tables 24
through 26. The control efficiency of the secondary crusher scrubber is
summarized in Table 27. Complete particulate results, including formulae
used in the calculations, are included in Appendix A. Field data sheets are
included in Appendix B.
TABLE 24
SUMMARY OF PARTICULATE RESULTS
Secondary Crusher Exhaust
Date:
Time Started:
Time Ended:
Run No.:
Gas Flow Rate, (dscfm):
Actual Gas Flow Rate,
(acfm):
Particulate Concen-
tration (gr/dscf):
Particulate Mass Flow,
(Ibs/hr):
TABLE
11-14-79
1425
1607
4
1750
2060
1.87
28.0
25
11-15-79
0845
0950
5
1850
2140
0.820
13.0
11-15-79
1115
1220
6
1830
2140
0.904
14.2
SUMMARY OF PARTICULATE RESULTS
Secondary Crusher Scrubber Inlet
Date:
Time Started:
Time Ended:
Run No. :
Gas Flow Rate, (dscfm):
Actual Gas Flow Rate,
(acfm):
Particulate Concen-
tration, (gr/dscf):
Particulate Mass Flow
Rate (Ibs/hr):
11-14-79
1415
1613
4
8270
9810
0.335
23.7
11-15-79
, 0830
0938
5
7880
9180
0.252
17.0
11-15-79
1105
1220
6
8250
9690
0.229
16.2
Scott Environmental Technology Inc.
-------
#2701-01-0280
-38-
TABLE 26
SUMMARY OF PARTICULATE RESULTS
Secondary Crusher Scrubber Outlet
Date:
Time Started:
Time Ended:
Run No.:
Gas Flow Rate, (dscfm):
Actual Gas Flow Rate,
(acfm):
Particulate Concen-
tration (gr/dscf):
Particulate Mass Flow
Rate (Ibs/hr):
11-14-79 11-15-79
1525 0757
1739 0956
4 5
22100 21700
25500 24900
0.0234 0.0116
4.4
2.1
11-15-79
1100
1256
6
21600
24900
0.0187
3.5
TABLE 27
SUMMARY OF CONTROL EFFICIENCY
Secondary Crusher.Scrubber
Run No. 12 3 Avg.
Control Efficiency («) 81.4 87.6 78.4 82.5
Gas flow and particulate mass flow rates in the duct exhausting the
feeder hoods (which was not sampled) can be determined by subtracting the flow
rates at the secondary crusher exhaust from the scrubber inlet. The particulate
concentration and particulate mass flow rate measured at the secondary crusher
exhaust during Run No. 1 appears high because it is somewhat higher than the
mass flow rate measured at the scrubber inlet during the same test run. There
was a large increase in gas flow volume between the scrubber inlet and the
scrubber outlet test locations. This increase averaged 194%.
' Scott Environmental Technolosy Inc.
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#2701-01-0230 -39-
Results of the particle size analyses at the secondary crusher are
summarized in Tables 28 through 34 and Figures 8 through 10. Field data
sheets are included in Appendix C.
Results of the visible emissions observations are summarized in
Tables 35 through 49. These results show no visible emissions at the conveyor
i
tunnel outlet, 0 to 5% opacity emissions at the reclaim feeder hood, and
0 to 10% opacity emissions at the secondary crusher exhaust hood. No visible
emissions were noted at the scrubber outlet. Field data sheets are included
in Appendix D.
3.3 TRUCK LOADOUT
Particulate sampling at the truck loadout facility was conducted
in the duct exhausting the conveyor belt loading ore into railroad cars, in
the duct exhausting the truck loadout hood, and at the baghouse outlet. Visible
emissions were monitored at the truck loadout hood, the conveyor hood, the
railroad car loading chute, and the baghouse outlet.
Results of the particulate testing are summarized in Tables 50 through
52. The control efficiency of the baghouse is summarized in Table 53. Complete
particulate results, including formulae used in the calculations, are included
in Appendix A. Field data sheets are included in Appendix B.
3.4 TRACE ELEMENT ANALYSIS
Particulate samples from two Method #5 tests were subjected to an
analysis for trace elements. Results of the analyses conducted are presented
in Appendix F. The samples analyzed are as follows:
o Secondary Crusher Scrubber Inlet - Run 6
- Sample #37692
o Truck Loadout Conveyor Exhaust - Run 9
- Sample #37693
An attempt was made to conduct a trace element analysis of the
particle samples from the Primary Crusher Conveyor Belt, Run 3, however
sufficient sample was not available for the analysis.
Scott Environmental Technology Inc
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#2701-01-0280
-40-
TABLE*28
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-15-79
Time: 0805
Sampling Location:
Traverse Point No,
Run No.:,' 4
Secondary Crusher Ex-
Sampled: 3 haust
Pbar(in. Hg): 26.41
Stack Temp. (°F): 67.0
Sample Time (Min): 20
Sample Volume (cf): 16-02
Moisture (% H?0): 1-7
Meter Temperature ( F): 68.0
Flow Setting, All (in. O): 1-85
Nozzle Diameter (In.): -196
Sample Flow Rate (at stack conditions) - .81 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
390. 202
7.00
4.80
4.60
4.40
5.00
1.00
.40
%
93.48
1.67
1.14
1.10
1.05
1.19
.23
.09
Back-up
Filter
.00
.00
Cumulative
%
100.00
6.51
4.83
3.68 .
2.58
1.53
.33
.09
ECD1
(Micrometers)
10.75 and
6.83
4.50
3.11
1.99
1.01
.61
.41
larger
.00
Total 417.40
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
: Scott Environmental Technology Inc
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#2701-01-0280
-41-
TABLE 29
PARTICLE SIZE DISTRIBUTION ANALYSIS
Traverse Point No.
Run No.: 5
Date: 11-15-79 p (in. Hg): 26.41
Time: ™^ cbar, T ,oc. fi7 n
Sampling Location: Secondary Crusher Exhausfwck Temp. F): 67.0
Tvav/orcp Pmnf Mn ^mniDH- 3 ^"P1 e Time (Mm): JO
0 Sample Volume (cf)- 8.52
Moisture (% H20):
Meter Temperature (UF):
Flow Setting, AH (in. O): 1-85
Nozzle Diameter (In.): -196
1.7
87.0
Sample Flow Rate (at stack conditions) - .86 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
441. 302
21.40
11.30
4.90
5.40
4.20
.60
.10
.00
90.20
4.37
2.30
1.00
1.10
.85
.12
.02
.00
Cumulative
%
100.00
9.79
5.41
3.10
2.10
1.00
.14
.02
ECD1 '
(Micrometers )
10.42 and
6.62
4.36
3.02
1.93
.98
.59
.39
larger
.00
<.39
Total
489.20
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technology Inc.
-------
#2701-01-0280 -42-
TABLE 30
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-15-79 P (in. Hg): 26.41
Time: 1240 <.:ar. ,on ,Q n
Sampling Location: Secondary Crusher Exhausttac.K '^mp- L '; ;
Traverse Point No. Sampled: 3 f mp e J'f (MJn); 5, ?n
R N ., 6 p Sample Volume (cf): 4.20
Run N°" b Moisture (% O): n 2.4
Meter Temperature ( F): 99.0
Flow Setting, AH (in. H?0): 1-75
Nozzle Diameter (In.): -196
Sample Flow Rate (at stack conditions) - .85 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 79.20* 47.48 100.00 10.47 and larger
2 40.60 24.34 52.51 6.66
3 27.20 16.30 28.17 4.39
4 12.70 7.61 'll.87 3.03
5 4.10 2.45 4.25 1-94
6 2.50 1.49 1.79 -99
7 .30 .17 .29 -59
8 .20 . .11 .11 -40
.00 .00 .00 <-41
Total 166.80
ECD - Effective Cutoff Diameter of preceding plate.
o
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scort Environmental Techndosy Inc
-------
#2701-01-0280
-43-
TABLE 31
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-15-79 p (in. Hg): 26.37
Time: 0755 ™J\ ,0. gl Q
Sampling Location: Secondary Crusher Scrubber^ '::TP' }...': iA
Traverse Point No. Sampled: 3 Inlet Samp e Time (Mm): 20
P No . 4 Sample Volume (cf): 21.68
Run N°" * Moisture (X HO): 1.2
Meter Temperature ( F): 61.0
Flow .Setting, AH (in. H?0): 3.20
Nozzle Diameter (In.): .250
Sample Flow Rate (at stack conditions) - 1.09 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
175.20^
43.50
18.30
8.90
6.90
4.. 40
.00
.00
%
68.11
16.91
7.11
3.46
2.68
1.71
.00
.00
Back-up
Filter
.00
.00
Cumulative
%
100.00
31.88
14.96
7.85
4.39
1.71
.00
.00
.00
ECD1
(Micrometers)
9.19 and larner
5.87
3.86
2.66
1.70
.86
.52
.34
Total
257.20
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
| Scott Environmental Technology Inc.
-------
#2701-01-0280
-44-
TABLE 32
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-15-79
Time: 1050
Sampling Location: Secondary Crusher Scrubb
Traverse Point No. Sampled: 3 Inlet
Run No.: 5
30 Tmp'
26.43
.08
Moisture (% O): 1.3
Meter Temperature ( F):
Row Setting, AH' (in. H?0): 3.20
Nozzle Diameter (In.): -250
90.0
Sample Flov/ Rate (at stack conditions) - 1.13 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(ing)
104. OO2
22.30
11.10
7.00
5.00
2,30
.20
.10
%
68.42
14.67
7.30
4.60
3.28
1.51
.13
.06
Back-up
Filter
.00
.00
Cumulative
%
100.00
31.57
16.90
9.60
5.00
1.71
.19
.06
ECD1 ' .
(Micrometers )
9.08 and larger
5.80
3.81
2.63
1.68
.85
.51
.34
.00
£.34
Total 152.00
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technofosy Inc.
-------
#2701-01-0280 -45~
TABLE 33
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-15-79 p (in. Hg): 26.43
Time: 0130 . ' jar
Sampling Location: Secondary Crusher Scrubb^ck Temp. F): 66.0
Traverse Point. No. Sampled: 3 Inlet Samp e Time (Mm): 5
R N 6 SamPle Volume (cf): 5.53
Run N°" Moisture (% H90): n 1.3
Meter Temperature ( F): 100-0
Flow Setting, AH (in. O): 3-20
Nozzle Diameter (In.): d .250
Sample Flow Rate (at stack conditions) - 1.13 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 49.002 59.75 100.00 9.09 and larger
2 12.80 15.60 40.24 5.81
3 8.30 10.12 24.63 3.81
4 5.30 6.46 14.51 . 2.64
5 3.60 4.39 8.04 1.68
6 1.70 2.07 3.65 .85
7 .20 .24 1.58 ' .51
8 .50 .60 1.34 .34
Back-up 6Q ?3 ?3 . 34
mter -bU .16 .16 <.^
Total 82.00
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technotosy Inc.
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#2701-01-0280 -46-
TABLE 34
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-15-79 P (in. Hg): 26.39
Time: 1334 &ar 0 KK n
Sampling Location: Secondary Crusher Scrubt^k Temp. F): 65.0
Traverse Point No. Sampled: 3 Outlet Samp e Time (Mm): f
P N . 6 Sample Volume (cf : 62.28
Run N°" Moisture (% H,0): 2.5
Meter Temperature ( F): 104.0
Flow.Setting, AH (in. O): I-25
Nozzle Diameter (In.): -273
Sample Flow Rate (at stack conditions) - .70 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 21.202 86.53 100.00 11.54 and larger
2 .20 . .81 13.46 7.31
3 .30 • 1.22 12.65 4.83
4 .30 1.22 11.42 ,' . 3.34
5 .60 2.44 10.20 2.13
6 1.00 4.08 7.75 1.09
7 .80 3.26 3.67 .66
8 .10 .40 .40 .44
Back-up
Filter -°° -°° -°° ^'44
Total 24.50
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
\ Scott Environmental Technology Inc.
-------
4 *t *ul KEurrilu ft L'l-s
O.iA'l' ' Ii .1'C
:n no.
2 CYCi.ro
90.99
0.2 0.1 O.OS
0.01
-------
Hhjtt-99-99
0.01
RUN 5 H Q
RUN 6 A A
iiiiiritiiiMini
.i_.
0 01
Cumulative %, Less Than Stated
Particle Size
nTrrririTnMiTrmTm'rnTTrniiiiiiiiii
'> HI ?0 jQ '.O 50 r,J '/!)
'Mill
IIMII
-
:.-.
_.
— -
i
i
1
!
1
i
i
i
-
—
—
HO
'is ca
-------
5v
£_ KtUFrLL ft
5SEH CC.
2 CYCLEH
taAUC IN U.S.A.
99.99
99.9 99.8
0.2 O.i. 0.05
0.01
FIGURE 10
SECONDARY CRUSHER SCRUBBER OUTLET
RUN 6
Cumulative %, Less Than Stated
Particle Size
TrmniirrmrrmTniTiiin
-------
#2701-01-0280
-50-
TABLE 35
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Tunnel Outlet
Test Run No.: 4
Date: 11-14-79
Color of Plume: White
Stack Height: 6 ft.
Distance to Stack: 15 ft.
Wind Direction: SE Speed: 0-5
Sky Description: Partly Cloudy
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
Overall
Time
Start -End
1420
1426
1432
1438
1444
1450
1456
1502
1508
1514
1533
1539
1545
1551
1557
1603
1609
1615
1621
1627
1645
1651
1657
1703
1709
Average
1426
1432
1438
1444
1450
1456
1502
1508
1514
1520
1539
1545
1551
1557
1603
1609
1615
1621
1627
1633
1651
1657
1703
1709
1715
- 0
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
' 0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
• o
0
0
0
0
0
0
0
0
0
0
Set Time Opacity
Number Start End Sum Averaae
'
' Scoa Environmental Techndosy Inc.
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#2701-01-0280
-51-
TABLE 36
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Tunnel Outlet
Test Run No.: 5
Date: 11-15-79
Color of Plume: White
Stack Height: 6 ft.
Distance to Stack:. 15 ft-
Wind Direction: SE Speed:
Sky Description: Clear
0-2
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Overall
Time
Start
0802
0808
0814
0820
0826
0832
0838
0844
0850
0905
0911
0917
0923
0929
0935
0941
0947
0953
0959
Average
End
0808
0814
0820
0826
0832
0838
0844
0850
0856
0911
0917
0923
0929
0935
0941
0947
0953
0959
1005
- 0
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0'
0
0
0
0
0
. 0
0
0
0
0
Set Time Opacity
Number Start End Sum Averaae
-
: Scon Environmental Technokxsy Inc.,
-------
#2701-01-0280
-52-.
TABLE 37
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Tunnel Outlet
Test Run No.: 6
Date: 11-15-79
Color of Plume: White
Stack Height: 6 ft.
Distance to Stack: 15 ft.
Wind Direction: SE Speed: 3-7
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Overall
Time
Start
1100
1106
1112
1118
1124
1130
1136
1142
1148
1154
1205
1211
1217
1223
1229
1235
1241
1247
1253
1259
Average
End
1106
1112
1118
1124
1130
1136
1142
1148
1154
1200
1211
1217
1223
1229
1235
1241
1247
1253
1259
1305
- 0
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. o
0
0
0
0
0
Set Time Opacity
Number Start End Sum Averaae
'
.
1 Scott Environmental Technology Inc.
-------
#2701-01-0280 -53-
TABLE 38
SUMMARY OF FUGITIVE EMISSIONS
Date: 11-14-79 11-15-79 11-15-79
Location: Secondary Crusher
n ., Tunnel Outlet „ r A
Run No.: 4 5 6
Time Started: 1420 0802 1100
Time Ended: 1717 1005 1305
Test Duration (seconds): 9120 7200 7200
Cumulative Duration of
Emissions (seconds): 000
Percentaqe of Test Duration with
Emissions (%): 0 0 0
Average (Percent): 0
' Scott Environmental Technology Inc.
-------
#2701-01-0280
-54-
TABLE 39
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Reclaim Feeder Stack Height: 1 ft.
Test Run No.: 4 Distance to Stack: 7 ft.
Date: 11-14-79
Color of Plume:
White
Wind Direction: N/A Speed:
Sky Description: Indoors
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
flvpral 1
Time
Start End
1420
1426
1432
1438
1444
1530
1536
1542
1548
1554
1600
1606
1612
1618
1624
1630
1636
1642
1648
1654
1700
1706
1712
1718
1724
Avpracip
1426
1432
1438
1444
1450
1536
1542
1548
1554
1600
1606
1612
1618
1624
1630
1636
1642
1648
1654
1700
1706
1712
1718
1724
1730
- n
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
• o
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
• 0
0
0
0
0
0
0
0
0
0
0
Set Time ' Opacity
Number Start End Sum Averaae
,
1 Scott Environmental Technokyjy Inc.
-------
#2701-01-0280
-55-
TABLE 40
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Feeder Hood
Test Run No.: 5
Date: 11-15-79
Color of Plume: White
Stack Height: 7 ft. horizontal
Distance to Stack: 10 ft.
Wind Direction: N/A Speed:
Sky Description: Indoors
Set
Number
1 -
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Overall
Time
Start
0800
0806
0812
0818
0824
0830
0836
0842
0848
0854
0900
0906
0912
0918
0924
0930
0936
0942
0948
0954
Average
End
0806
0812
0818
0824
0830
0836
0842
0848
0854
0900
0906
0912
0918
0924
0930
0936
0942
0948
0954
1000
- 0
Sum
0
80
20
10
65
70
35
5
5
0
0
10
15
30
30
15
35
0
0
0
Opacity
Average
0
5
0
0
5
5
0
0
0
0
0
0
0
0
. 0
0
0
0
0
0
Set Time Opacity
Number Start End Sum Averaae
; Scott Environmental Technobsy Inc.
-------
#2701-01-0280
-56-
TABLE 41
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Feeder Hood
Test Run No.: 6
Date: 11-15-79
Color of Plume: White
Stack Height: 7 ft.
Distance to Stack: 10 ft.
Wind Direction: N/A Speed:
Sky Description: Indoors
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Overall
Time
Start End
1115
1121
1139
1145
1151
1157
1203
1209
1215
1221
1227
1233
1239
1245
1251
Average
1121
1127
1145
1151
1157
1203
1209
1215
1221
1227
1233
1239
1245
1251
1257
- 0
Sum
0
35
0
0
0
0
0
0
0
0
0.
0
15
15
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
• 0
Set Time Opacity
Number Start End Sum Averaae
-
! Scott Environmental Technobsy Inc.
-------
#2701-02-0280
-57-
TABLE 42
SUMMARY OF FUGITIVE EMISSIONS
Date: 11-14-79 11-15-79 11-15-79
Location: Secondary Crusher
,. ., Feeder Hood . r /-
Run No.: 4 5 b
Time Started: 1420 0805 1120
Time Ended: 1730 0945 1255
Test Duration (seconds): ' 9000 5408 5130
Cumulative Duration of
Emissions (seconds): 0 913 352
Percentage of Test Duration with
Emissions (%): 0 16.9% 6.9%
Average (Percent): 7.9%
; Scott Environmental Technology Inc.
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#2701-01-0280
-58-
TABLE 43
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Exhaust
Test Run No.: 4
Date: '11-14-79
Color of Plume: White
Stack Height: 6 ft.
Distance to Stack: 20 ft.
Wind Direction: East Speed: 5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Overall
Time
Start
1412
1418
1424
1430
1436
1449
1455
1501
1507
1531
1537
1543
1549
1555
1610
1617
1623
1629
1635
Average
End
1418
1424
1430
1436
1442
1455
1501
1507
1513
1537
1543
1549
1555
1601
1617
1623
1629
1635
1641
- 5
Opacity
Sum
170
115
100
135
170
130
180
165
170
30
30
50
5
40
45
45
60
40
20
Average
5
5
5
5
5
5
10
5
5
0
0
0
0
0
. 0
0
0
0
0
Set Time Opacity
Number Start End Sum Averacie
•
-
: Scott Environmental Technology Inc.
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#2701-01-0280
-59-
TABLE 44
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Exhaust
Test Run No.: 5
Date: 11-15-79
Color of Plume: White
Stack Height: 6 ft.
Distance to Stack:. 20 ft.
Wind Direction: East Speed: 5
Sky Description: Clear
Set
Number
1 -
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Overall
Time
Start
0802
0808
0714
0820
0826
0838
0844
0850
0856
0902
0920
0926
0932
0938
0944
0950
Average
End
0808
0814
0820
0826
0832
0844
0850
0856
0902
0908
0926
0932
0938
0944
0950
0956
- 5
Opacity
Sum
110
105
115
120
115
105
110
140
225
180
110
75
105
45
35
115
Average
5
5
5
5
5
5
5
5
10
10
5
5
5
0
• 0
5
Set Time Opacity
Number Start End Sum Averaae
i Scott Environmental Technolosy Inc
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#2701-01-0280
-60-
TABLE 45
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Exhaust
Test Run No.: 6
Date: 11-15-79
Color of Plurne: White
Stack Height: 6 ft.
Distance to Stack: 20 ft.
Wind Direction: East Speed: 5 mPn
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Overall
Time
Start
1104
1110
1116
1122
1128
1145
1151
1157
1203
1209
1225
1231
1237
1243
1249
Average
End
1110
1116
1122
1128
1134
1151
1157
1203
1209
1215
1231
1237
1243
1249
1255
- 5
Opacity
Sum
170
135
160
175
170
155
110
165
170
130
155
120
15
65
5
Average
5
5
5
5
5
5
5
5
5
5
5
5
0
0.
•0
Set Time Opacity
Number Start End Sum Averaae
"-.
'
Scott Environmental Technolosy Inc
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#2701-01-0280 ,,
-bl-
TABLE 46
SUMMARY OF FUGITIVE EMISSIONS
'Date: 11-14-79 11-15-79 11-15-79
Location: Secondary Crusher Exhaust
Run No.: 4 5 6
Time Started: 1412 0802 1104
Time Ended: 1640 0958 1257
Test Duration (seconds): 6278 5870 4920
Cumulative Duration of
Emissions (seconds): 4686 5223 3784
Percentage of Test Duration with
Emissions (%): . 74.6% 89.0% 76.9%
Average (Percent): 80.2%
(\) Scotr Environmental Technology Inc
-------
#2701-01-0280
-62-
TABLE 47
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Baghouse Outlet
Test Run No.: 4
Date: 11-14-79
Color of Plume: White
Stack Height: 50 ft.
Distance to Stack: 50 ft.
Wind Direction: South Speed: °~5
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Overall
Time
Start End
1533
1539
1545
1551
1557
1603
1609
1615
1621
1627
1633
1639
1645
1651
1657
1703
1709
Average
1539
1545
1551
1557
1603
1609
1615
1621
1627
1633
1639
1645
1651
1657
1703
1709
1715
- 0
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. 0
0
0
Set Time Opacity
Number Start End Sum Averaae
: Scott Environmental Technology Inc.
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#2701-01-0280
-63-
TABLE 48
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Baghouse Outlet Stack Height: 50 ft.
Test Run No.: 5 Distance to Stack: 30 ft.
Date: 11-15-79 Wind Direction: South Speed: 0-5
Color of Plume: White Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Time
Start
0804
0810
0816
0822
0828
0834
0840
0846
0852
0858
0914
0920
0926
0932
0938
0944
0950
0956
1002
End
0810
0816
0822
0828
0834
0840
0846
0352
0858
0904
0920
0926
0932
0938
0944
0950
0956
1002
1008
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. 0
0
0
0
0
Set Time Opacity
Number Start End Sum Averaae
; Scott Environmental Technofosy Inc.
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#2701-01-0280
-64-
TABLE 49
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Secondary Crusher Baghouse Outlet stack Height: 50 ft.
Test Run No.: 6 Distance to Stack: 30 ft.
Date: 11-15-79 Wind Direction: South Speed: 0-5
Color of Plume: Wnite • Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
Overall
Time
Start End
1110
1116
1122
1128
1134
1140
1146
115?
1158
1204
1210
1216
1222
1228
1234
1240
1246
1252
Average
1116
1122
1128
1134
1140
1146
1152
1158
1204
1210
1216
1222
1228
1234
1240
1246
1252
1258
- 0
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. 0
0
0
0
Set Time Opacity
Number Start End Sum Averaae
; Scon Environmental TechnoJogy Inc
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#2701-01-0280 -65-
TABLE 50
SUMMARY OF PARTICULATE RESULTS
Truck Loadout Conveyor Exhaust
Date: 11-16-79 11-17-79 11-17-79
Time Started: 1155 0800 1203
Time Ended 1403 1055 1450 *
Run No.: 789
Gas Flow Rate, (dscfm): 1130 1180 1130
Actual Gas Flow Rate,
(acfm): 1320 1370 1320
Particulate Concen-
tration, (gr/dscf): 0.604 0.491 1.00
Particulate Mass Flow . -
Rate, (Ibs/hr): 5.9 5.0 9.7
Scott Environmental Technology Inc.
-------
#2701-01-0280 -66-
TABLE 51
SUMMARY OF PARTICULATE RESULTS
Truck Loadout Hood Exhaust
Date: 11-16-79 11-17-79 11-17-79
Time Started: 1155 0800 1200
Time Ended: 1405 1100 1450
Run No.: 7 8 9
Gas Flow Rate, (dscfm): 1540 1580 1550
Actual Gas Flow Rate,
(acfm): 1780 1810 1780
Particulate Concen-
tration, (gr/dscf): 0.0556 0.0288 0.0098
Particulate Mass Flow
Rate, (Ibs/hr): 0.73 0.39 0.12
TABLE 52 .
SUMMARY OF PARTICULATE RESULTS
Truck Loadout Baghouse Outlet
Date: 11-16-79 11-17-79 11-17-79
Time Started: 1200 0804 1203
Time Ended: 1414 1101 1546
Run No.: 789
Gas Flow Rate (dscfm): 2530 2690 2550
Actual Gas Flow Rate,
(acfm): 2950 3100 2990
Particulate Concen-
tration, (gr/dscf): 0.0088 0.0158 0.0153
Particulate Mass Flow
Rate, (Ibs/hr): 0.18 0.36 0.33
I (\)' Scott Environmental Technology Inc.
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#2701-01-0280 -67-
TABLE 53
SUMMARY OF CONTROL EFFICIENCY
Truck Loadout Baghouse
Run No.: 123 Avg.
Control Efficiency (%): 97.2 93.7 96.6 95.8
The mass flow rates at the conveyor exhaust and the loadout hood
exhaust were added together to determine the baghouse inlet mass flow rate.
Due to time limitations, only two particle size analyses samples
were collected at both the conveyor exhaust and the loadout hood exhaust. No
samples were collected at the baghouse outlet. Results of the particle size
analyses are presented in Tables 54 through 57 and Figures 11 and 12. .
Field data sheets are included in Appendix C.
Results of the visible emissions observations at the loadout hood,
the conveyor exhaust hood, the railroad car loading chute, and the baghouse
outlet are summarized in Tables 58 through 71. These results show 0% average
opacity at the loadout hood, 0 to 25% opacity at the conveyor exhaust hood, and
0 to 5% opacity at the railroad car loading chute. Field data sheets are
included in Appendix D.
The weight of ore concentrate unloaded by each truck during the test
period was recorded and is included in Table 72.
Scott Environmental Technology Inc.
-------
#2701-01-0280 _68_
TABLE 54
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-16-79 PK^(in- H9): 26-31
Timo- 1 RDR Dai
Sampling LocationJruck Loadout Conveyor Stack Temp. ( F): 76.0
Traverse Point No. Samoled: 3 Exhaust^P e Time (Mm): 13.9
P Nn . 7 ' Sample Volume (cf): 12.96
Run NO" ' Moisture (% H?0): -2
Meter Temperature ( F): 77.0
Flow-Setting, AH (in. O): 2.40
Nozzle Diameter (In.): ^ .210
Sample Flow Rate (at stack conditions) - .93 cfm
ECD1 '
(Micrometers )
10.08 and larger
6.42
4.23
2.92
1.87
.95
.57
.38
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
208.80
56.00
32.40
13.90
5.30
2-. 90
.40
.20
*
65.18
17.48
10.11
4.33
1.65
.90
.12
.06
Cumulative
100.00
34.81
17.32
7.21
2.87
1.21
.31
.18
Fi?terP -40 -12 -12
Total 320.30
ECD - Effective Cutoff Diameter of preceding plate.
o
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
! Scott Environmental Technology Inc.
-------
#2701-01-0280
-69-
TABLE 55
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date:
Time:
11-17-79
1149
Pbar(in. Hg): 26.14
nme' ii^y — .0
Sampling Location: Truck Loadout Conveyor $tac!< Te.mP- MF': 62,-°
Travpr*; Pnint Nn. Samnlprt- 3 Exhaust SamPle Tlme (Ml.n).: 7'8
Traverse Point No.
Run No.: 8
Sampled: 3 Exhaust
83
Sample Volume (cf): 8.09
Moisture (% H?0): 2.1
Meter Temperature ( F): 70.0
Flow.Setting, AH (in. H?0):2.80
Nozzle Diameter (In.): -210
Sample Flow Rate (at stack conditions) - 1.05 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
267.50
104.90
127.60
58.50
20.60
5-. 40
.70
.50
%
45.60
17.88
21.75
9.97
3.51
.92
.11
.08
Cumulative
100.00
54.39
36.50
14.74
4.77
1.26
.34
.22
ECD1
(Micrometers )
9.38 and larger
5.99
3.94
2.72
1.74
.88
.53
.35
Back-up
Filter
.80
.13
.13
<.35
Total
586.50
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
j Scott Environmental Technology Ire
-------
#2701-01-0280
-70-
TABLE 56
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-16-79
Time: 1701
Sampling Location: Truck Loadout Exhaust
Traverse Point No. Sampled: B-4 Hood
Run No.:/7
Pbar(in. Hg): 26.31
Stack Temp. (°F): 73.0
Sample Time (Min): 35
Sample Volume (cf): 43.16
Moisture (% H?0): .4
Meter Temperature ( F): 90.0
Flow Setting, AH (in. O): 4-10
Nozzle Diameter (In.): -250
Sample Flow Rate (at stack conditions) - 1.22 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
91.00
40.60
39.80
24.00
8.60
5,00
.90
1.10
%
42.68
19.04
18.66
11.25
4.03
2.34
.42
.51
Cumulative
100.00
57.31
38.27
19.60 .
8.34
4.31
1.96
1.54
ECD-
(Micrometers)
8.73 and larger
5.59
3.67
2.53
1.62
.82
.49
.32
Back-up
Filter
2.20
1.03
1.03
<.32
Total
213.20
1
ECD - Effective Cutoff Diameter of preceding plate.
Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
j{y); Scott Environmental Technobsy Inc.
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#2701-01-0280
-71-
TABLE 57
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 11-17-79
Time: 1550
Sampling Location: Truck Loadout Exhaust
Traverse Point No. Sampled: B~4 Hood
Run No.: 8
Pbar(in. Hg): 26.14
Stack Temp. (°F): 59.0
Sample Time (Min):7
Sample Volume (cf): 9.48
Moisture (% H?0): 1.2
Meter Temperature ( F): 70.0
Flow. Setting, AH (in. O): 4.20
Nozzle Diameter (In.): ^ -250
Sample Flow Rate (at stack conditions) - 1.32 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt.
(mg)
38.10
1.60
1.50
.70
.30
•.40
.20
.00
%
89.01
3.73
3.50
1.63
.70
.93
.46
.00
Cumulative
%
100.00
10.98
'7.24
3.73
2.10
1.40
.46
.00
ECD1 '
(Micrometers)
8.33 and larger
5.34
3.50
2.42
1.55
.78
.47
.31
.00
.00
£.31
Total
42.80
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
I (Jy! Scott Environmental Technofosy Inc.
-------
• r, n^^^Wl.
2 CYCLES
99-39
99 98
95
90
60 50
0.01
-------
caann co.
Z CYCLES
99.99
99.9 99.0
99 98
95
90
80 70 GO 50 40 30
20
10
0.5 0.? 0.1 0.05
0.01
10
9
8
7
G
i_^ >
Li.
4TP
0 i
n4!
,5.
.4_
,3_.
.2_
*a
BJ
11
rr
H-
O
h-1
(B
C/5
H-
N
n>
icrometers
ILL
-FI
™p
-p
i
TT
•-1 -
-li'-L
u.
\r\
-
1
TTu
i-ifi.
! lit
44-i'
'Ml
E
V-
i
11
TR
IF
HI
TTT
la
1
L
Tl
i.!.
l i
Ml!.
•
ji
-ii
.-.
TI
!
iT
t
n"n"
T
L-r
| |
!
i :
~r~r
•i-
lUi
L:
E
: i_u
LH-
•
il 1
i ! - lo-
till
inn
OJ
_ I .
n-
FIGURE 12
TRUCK LOADOUT EXHAUST HOOD
RUN 7 o O
RUN 8g QJ
riLiiiinn
Cumulative %, Less Than Stated
Particle Size
-------
#2701-01-0280
-74-
TABLE 58
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Hood
Test Run No.: 7
Date: 11-16-79
Color of Plume: Uhite
Stack Height: 15 ft.
Distance to Stack: 25 ft.
Wind Direction: NE Speed: 10
Sky Description: Clear
Set Time Opacity
Number Start End Sum Average
1 - 1157
2 1219
3 1318
4 1324
5 1331
6 1341
7 1355
8 1409
Overall Average
1203 45 0
1225 15 0
1324 0 0
1330 10 0
1337 5 0
1347 20 0
1401 15 0
1415 10 0
- 0
Set Time Opacity
Number Start End Sum Averaae
1 -
; Scott Environmental Technology Inc.
-------
#2701-01-0280
-75-
TABLE 59
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Hood
Test Run No.: 8
Date: 11-17-79
Color of Plums: White
Set Time Opacity
Number Start End Sum Average
1 • 0803 0809 35 0
2 0817 0823 45 0
3 0828 0834 40 0
4 0902 0908 25 0
5 1000 1006 35 0
6 1026 1032 15 0
7 1050 1056 20 0
Overall Average - 0
Set Time
Number Start End
Stack Height: 15 ft.
Distance to Stack: 25 ft.
Wind Direction: NE Speed: 5
Sky Description: Overcast
Opacity
Sum Averaae
; Scott Environmental Technology Inc.
-------
#2701-01-0280
-76-
TABLE 60
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Hood
Test Run No.: 9
Date: 11-17-79
Color of Plume: White
Stack Height: 15 ft.
Distance to Stack: 25 ft.
Wind Direction: South Speed: 10-15
Sky Description: Partly Cloudy
Set Time Opacity
Number Start
1 1201
2 1210
3 1229
4 1312
5 1350
6 1356
7 1440
Overall Average
End Sum Average
1207 30 0
1216 20 0
1235 10 0
1318 10 0
1356 5 0
1402 25 0
1446 15 0
- 0
Set Time Opacity
Number Start End Sum Averaae
-
Scott Environmental Technokyjy Inc.
-------
#2701-01-0280
-77-
TABLE 61
SUMMARY OF FUGITIVE EMISSIONS
Date: 11-16-79 11-17-79 11-17-79
Location: Truck Loadout Hood
Run No.: 7 8.9
Time Started: 1158 0805 1202
Time Ended: 0220 1101 0252
Test Duration (seconds): 4380 4020 4020
Cumulative Duration of
Emissions (seconds): 3678 1734 1721
Percentage of Test Duration with
Emissions (%): 84.0% 43.1% 42.8%
Average (Percent): 56.6%
Scon Environmental Technology Inc.
-------
#2701-01-0280
-78-
TABLE 62
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Conveyor Hood
Test Run No.: 7
Date: 11-16-79
Color of Plume: Wnite
Stack Height: 3 ft.
Distance to Stack: 5 ft.
Wind Direction: NE Speed: 8-10
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
Overall
Time Opacity
Start End Sum Average
1158 1204 625 25
1219 1225 580 25
1318 1324 395 15
1324 1330 275 10
1330 1336 245 10
1336 1342 210 10
1342 13.48 190 10
1356 1402 100 5
1409 1415 170 5
Average - 15
Set Time Opacity
Number Start End Sum Averaae
; Scott Environmental Technolosy Inc
-------
#2701-01-0280
-79-
TABLE. 63
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Conveyor Hood
Test Run No.: 8
Date: 11-17-79
Color of Plume: White
Stack Height: 4 ft.
Distance to Stack: 10 ft.
Wind Direction: Speed
Sky Description: Overcast
Set Time . Opacity
Number Start
1 • 0805
2 0819
3 0829
4 0903
5 1001
6 1026
7 1032
8 1051
Overall Average
End Sum Average
0811 30 0
0825 40 0
0835 45 0
0909 95 5
1007 110 5
1032 45 0
1038 40 0
1057 75 5
- 0
Set Time Opacity
Number Start End Sum Averacie
Scott Environmental Technolcxjy Inc.
-------
#2701-01-0280
-80-
TABLE 64
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Conveyor Hood
Test Run No.: 9
Date: 11/17/79
Color of Plume: White
Stack Height: 4 ft.
Distance to Stack: 10 ft.
Wind Direction: SE Speed: 10-15
Sky Description: Partly Cloudy-Overcast
Set Time . Opacity
Number Start
1 • 1202
2 1208
3 1230
4 1312
5 1349
6 1355
7 1440
8 1446
Overall Average
End Sum Average
1208 115 5
1214 30 0
1236 55 0
1318 75 5
1355 55 0
1401 20 0
1446 20 0
1452 10 0
- 0
Set Time Opacity
Number Start End Sum Averaae
' Scott Environmental Technobsy Inc
-------
#2701-01-0280
-81-
"TABLE 650
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Railroad Car Loading Chute
Test Run No.: 7
Date: 11-16-79
Color of Plume: White
Stack Height: 20 ft.
Distance to Stack: 100 ft.
Wind Direction: E-SW Speed:5-8
Sky Description: Clear
Set Time Opacity
Number Start End Sum Average
1 - 1157 1203 50 0
2 1220 1226 50 0
3 1319 1325 125 5
4 1325 1331 85 5
5 1334 1340 15 0
6 1345 1351 15 0
7 1355 1401 90 5
Overall Average - 0
Set Time Opacity
Number Start End Sum Averaae
Scott Environmental Technology Inc.
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#2701-01-0280
-82-
TABLE 66
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Railroad Car Loading Chute
Test Run No.: 8
Date: 11-17-79
Color of Plume: White
Set Time Opacity
Number Start
1 " 0804
2 0819
3 0829
4 0903
5 1001
6 1026
7 1051
Overall Average
End Sum Average
0810 120 5
0825 110 5
0835 90 5
0909 75 5
1007 85 5
1032 100 5
1057 25 0
- 5
Set Time
Number Start End
-
Stack Height: 20 ft.
Distance to Stack: 100 ft.
Wind Direction: E Speed: Calm
Sky Description: Overcast
Opacity
Sum Averaae
I (\) Scon Environmental Technokyjy Inc
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#2701-01-0280
-83-
TABLE 67
SUMMARY OF RESULTS OF OPACITY READINGS
Location
Test Run
Date:
Color of
Set
Number
1
2
3
4
5
6
7
8
9
Overall
: Railroad Car Loading Chute stack Height: 20 ft.
No.: 9 Distance to Stack: 100 ft.
H'17'79 . Wind Direction: SW Speed: 5~1
Plume: White sky Description: Overcast
Time Opacity
Start End Sum Average
1202 1208 40 0
1208 1214 20 0
1214 1220 25 0
1230 1236 35 0
1312 1318 105 5
1349 1355 55 0
1355 1401 25 0
1440 1446 25 0
1446 1452 50 0
Average - 0
Set Time Opacity
Number Start End Sum Averaae
' Scott Environmental Technology Inc
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#2701-01-0280 -84-
TABLE 68
SUMMARY OF FUGITIVE EMISSIONS
Date: 11-16-79 11-17-79 11-17-79
Location: Railroad Car Loading Chute
Run No.: ' 7 8 9
Time Started: 1158 0805 1202
Time Ended: 1420 1101 1452
Test Duration (seconds): 4320 3960 4080
Cumulative Duration of
Emissions (seconds): 3429 3234 3037
Percentage of Test Duration with
Emissions (%): 79.4% 81.7% 74.4%
Average (Percent): 78.5%
Scon Environmental Technokxjy Inc.
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#2701-01-0280
-85-
TABLE
69
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Baghouse Outlet
Test Run No.: 7
Date: 11-16-79
Color of Plume: White
Stack Height: 75 ft.
Distance to Stack: 100 ft.
Wind Direction: NE Speed:
Sky Description:
5-10
Set Tin1
Number Start
1 1157
2 1219
3 1318
4 1324
5 1330
6 1336
7 1342
8 1354
Overall Average
e Opacity
End Sum Average
1203 0 0
1225 0 0
1324 0 0
1330 0 • 0
1336 0 0
1342 0 0
1348 0 0
1400 0 0
- 0
Set Time Opacity
Number Start End Sum Averaoe
•
Scon Environmental Technolosy '^
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#2701-01-0280 -84-
TABLE 68
SUMMARY OF FUGITIVE EMISSIONS
Date: 11-16-79 . 11-17-79 11-17-79
Location: Railroad Car Loading Chute
Run No.: 789
Time Started: 1158 0805 1202
Time Ended: 1420 1101 1452
Test Duration (seconds): 4320 3960 4080
Cumulative Duration of
Emissions (seconds): 3429 3234 3037
Percentage of Test Duration with
Emissions (%): 79.4% 81.7% .74.4%
Average (Percent): 78.5%
. {_$_} Scott Environ menta; Techndcxjy Inc.
-------
#2701-01-0280
-85-
TABLE 69
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Baghouse Outlet
Test Run No.: 7
Date: 11-16-79
Color of Plume: White
Stack Height: 75 ft.
Distance to Stack: 100 ft.
Wind Direction: NE Speed:
Sky Description:
5-10
Clear
Set Time Opacity
Number Start
1 1157
2 1219
3 1318
4 1324
5 1330
6 1336
7 1342
8 1354
Overall Average
End Sum Average
1203 0 0
1225 0 0
1324 0 0
1330 0 0
1336 0 0
1342 0 0
1348 0 0
1400 0 0
- 0
Set Time
Number Start End
Opacity
Sum Averaae
; Scott Environmental Technofosy Inc
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#2701-01-0280
-86-
TABLE 70
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Baghouse Outlet
Test Run No.: 8
Date: 11-17-79
Color of Plume: White
Set Tine Opacity
Number Start
1 0805
2 0820
3 0830
4 0904
5 1002
6 1027
7 1050
Overall Average
End Sum Average
0811 0 0
0826 0 0
0836 0 0
0910 0 0
1008 0 0
1033 0 0
1056 0 0
- 0
Set Time
Number Start End
*
Stack Height: 70 ft.
Distance to Stack: 100 ft.
Wind Direction: NW Speed: 0-5
Sky Description: Overcast
Opacity
Sum Averaae
: Scott Environmenta' Technology Inc.
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#2701-01-0280
-87-
TABLE 71
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Truck Loadout Baghouse Outlet
Test Run No.: 9
Date: 11-17-79
Color of Plume:
Stack Height: 70 ft.
Distance to Stack: 100 ft.
Wind Direction: NW Speed:
Sky Description: Overcast
Set
Number
1
2
3
4
5
6
7
8
9
Overall
- Time Opacity
Start End Sum Average
1200 1206 0 0
1206 1212 0 0
1212 1218 0 0
1218 1224 0 0
1224 1230 0 0
1313 1319 0 0
1349 1355 0 0
1355 1401 0 0
1439 1445 0 0
Average - 0
Set Time Opacity
Number Start End Sum Averaae
Scott Environmental Technology Inc
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#2701-01-0280
-88-
TABLE 72
WEIGHT OF ORE CONCENTRATE
UNLOADED BY TRUCKS DURING
TEST PERIODS
Test Run Truck
Date Number Number
11-16-79 7 3
5
11
6
10
3
9
11-17-79 8 3
5
15
6
3
15
5
9 6
9
15
5
6
Time of
Arrival
1155
1215
1313
1317
1320
1350
1400
0800
0810
0830
0900
1000
1020
1050
1200
1210
1225
1310
1435
Time of
Departure
1205
1225
1330
1340
1350
1405
1420
.0815
0830
0845
0915
1015
1025
1100
1210
1220
1243
1325
1455
Load Weight (Ibs)
48700
49800
49540
50130
50350
49170
49070
49430
49870
50380
48840
48500
49720
49570
49970
48840
49870
49680
50900
Scott Environmental Technology Inc.
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#2701-01-0280 -89-
4.0 SAMPLING AND ANALYTICAL PROCEDURES
4.1 EPA METHOD #1 - SELECTION OF SAMPLING LOCATION
The sampling locations were selected in accordance with EPA Method #1.
This method requires that the sampling location be a minimum of two stack diameters
downstream and a half a diameter upstream from any flow disturbances. This
method also allows the smallest stack diameter to be 12 inches. For rectangular
ducts, an equivalent duct size is calculated. The number of sampling points is
specified in the method depending upon the length of undisturbed flow upstream
and downstream from the sampling location. The number of sampling points varies
from 8 to 48.
Each sampling location was selected so as to provide the maximum length
of undisturbed flow upstream and downstream from the sampling locations and, thus,
the minimum number of required sampling points. The number of sampling points at
each location was then selected based on EPA Method #1 criteria.
The duct at the primary crusher conveyor exhaust is 10 inches in
diameter, which is less than the 12 inch minimum allowed by Method #1. However,
sampling was conducted at this location since no .other suitable locations were
available. A stack extension was installed at the primary crusher scrubber
outlet to provide the minimum upstream and downstream duct lengths. Sampling
was conducted at 48 points at this location.
The secondary crusher exhaust duct and all three ducts sampled at
the truck loadout facility are also less than the 12 inch minimum diameter.
However, no other suitable sampling locations were available. Cyclonic flow
was encountered at the secondary crusher scrubber outlet. The angle of flow
was approximately 30 inches from vertical. The pitot and sampling nozzle were
rotated so as to face directly into the maximum gas flow.
4.2 EPA METHOD #2 - MEASUREMENT OF GAS VOLUME FLOW RATE
The gas volume flow rate was measured at each sampling location in
accordance with EPA Method #2. This method uses a Type S Pitot tube and an
inclined manometer to measure the velocity pressure, and a thermocouple to
measure gas temperature at each sampling point.
Preliminary velocity measurements were made at each sampling location
followed by velocity measurements as a part of each particulate test run.
The Pitot tubes used are within the dimensional limitations of
Method #2. A calibration factor of 0.834 was used for the Pi tots. A dry gas
r
Scott Environmental Techndcxjy Inc.
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#2701-01-0280 -90-
molecular weight of 28.84 was used at each location since, none of the processes
tested involved combustion cf fuel.
4.3 DETERMINATION OF MOISTURE CONTENT OF STACK GASES
Moisture content of the gases sampled was determined in accordance
with EPA Method #4 as part of the particulate sampling train. Moisture in the
gas sampled was collected in impingers in an ice bath followed by silica gel.
The moisture collected was then measured volumetrically and gravimetrically.
4.4 DETERMINATION OF PARTICULATE EMISSIONS
Particulate emissions were measured in accordance with EPA Method #5.
This method involves the isokinetic extraction of a sample from the gas stream
and collection of the particulate on a heated out-of-stack filter. A dry gas
meter measures the volume of the gas sample. Figure 13 shows a diagram of the
sampling train.
4.5 DETERMINATION OF VISIBLE EMISSIONS
Visible emissions were monitored by determining the smoke density using
EPA Method #9, and by determining fugitive emissions using EPA Method #22.
Method #9 involves the measurement of smoke density by a smoke reader who has
been previously certified against smoke measured by an opacity meter calibrated
with neutral density filters. Method #22 involves the determination of the
cumulative time fugitive emissions are visible during a given test period. The
density of the emissions is not recorded and the measurements may be made with
a non-certified reader.
4.6 DETERMINATION OF PARTICLE SIZE
The samples for particle size distribution at each sampling location
were collected using an Andersen 2000 cascade impactor. The particles are
collected by impaction on a series of plates. The plates have increasingly
smaller holes so that the velocity of the particles is increased from plate to
plate and smaller and smaller particles are impacted. The particulate weight
collected on each plate is determined gravimetrically. The particle size distri-
bution is based on the equivalent aerodynamic size of the particles based on
spherical particles of 1 gram/cc density.
Sampling and calculations of results were performed in accordance with
the operating manual published by Andersen 2000. Figure 14 shows a diagram of
the sampling train. The impactor was used out-of-stack at the inlet sampling
locations due to the small diameter of these ducts. For this arrangement, a
short probe was installed between the nozzle and the cascade impactor.
Scott Environmental Technology Inc.
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I
it
. tr
itf=£
<^^.
LEGEND;
1. NOZZLE
2. PROBE
3. PITOT
4. THERMOCOUPLE
5. PYROMETER
W-k-T-C^r-ti^D
Wj
20
6. INCLINE MANOMETER
7. CYCLONE
8. FLASK
9. FILTER ASSEMBLY
10. FILTER BOX
II. IMPINGER ICEBATH
12. IMPINGERS
13. THERMOMETER
U. CHECK VALVE
15. UMBILICAL CORD
16. VACUUM GAUGE
=«=
ro
i
o
ro
00
o
17,
18.
19.
20.
21.
COARSE FLOW ADJUST
VALVE
FINE FLOW ADJUST
VALVE
VACUUM PUMP
DRY TEST METER
ORIFICE TUBE
22. SOLENOID VALVES
FIGURE 13 - PARTICULATE SAMPLING TRAIN
-------
tr
1 3
rss
«^j
O
I
o
ro
CO
o
ro
i
LEGEND:
1. NOZZLE
2. PROBE
3. ANDERSEN CASCADE IMPACTOR
4. INCLINE MANOMETER
5. IMPINGER ICEBATH
6. IMPINGERS
7. THERMOMETER
8. CHECK VALVE
9. UMBILICAL CORD
10. VACUUM GAUGE
11. COARSE FLOW ADJUST
VALVE
12. FINE FLOW ADJUST
VALVE
13. VACUUM PUMP
14. DRY TEST METER
15. ORIFICE TUBE
16. SOLENOID VALVES
FIGURE .14. - PARTICLE SIZE DISTRIBUTION
SAMPLING TRAIN
-------
#2701-01-0280 . -93-
APPENDIX A
COMPLETE PARTICULATE RESULTS
INCLUDING FORMULAE USED
IN THE CALCULATIONS
Scott Environmental Techndosy Inc
-------
rnmary Irusner
Primary Crusher
. Location: -94- Conveyor Exhaust Surge Bin Exhai
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: P. (in. Hg.)
Static Pressure: P (in. O)
Area of Stack: A (ft2)
Pi tot Coefficient: C
Meter Calibration- Factor: Y
Area of Nozzle: A (in )
Total Sampling Time: "(Min.)
Gas Sample Volume: Vm (ft3)
Avg. Velocity Head: (V"Tp )svg. (in. O)
Avg. Orifice Pressure: AH (in HpO)
Avg. Stack Temperature: T (°R)
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: V (ml.)
Gas Sample Volume @ Std. Cond.:
Vm(Std) (ft3) = 17.64 VrnY (P, +&H/13.6)
Tm tar
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 YJc
Moisture Content: B = s Vw(Std)
Wj - Vm(Std) + Vw(Std)
Molecular Weicht of Stack Gas (dry):
Md = 0.44 (% C02) + 0.32 (% 02) +
0.28 (% N2+Z CO)
1
2
3
11-13-79
0923
1033
27.14
-4.8
0.545
0.834
1.00
0.0302
56
37.38
0.62
1.1
521
539
14
33.30
0.66
0.019
28.84
1335
1448
27.06
-4.8
0.545
0.834
1.00
0.0302
56
36.955
0.68
1.1
528
546
7
32.40
0.33
0.010
28.84
_1700
1820
..27.08
-4.8
0.545
0.834
1.00
0.0302
56
55.655
2.3
2.9
528
557
11
48.11
0.52
0.011
28.84
1
11-
r «Hil m* ill 1 JiB »l 1
0915
1020
27.16
-5.1
1.07
j
0.834
1.00 .
0.0491
60
41.108
0.31
1.32
521
552
9
35.81
0.42
0.012
28.84
> |
13-79
1340
""~144!f
27.06
-5.1
1.07-
0.834
1.00
0.0491
60
41.63
0.31
1.3
527
557
17
35.80
0.80
0.022
28.84
±!
1838*1
_^|
27.08
f'
1.07 *
0.834
A.uu
0.0491
60 -
41.82P
0.30 |
1.28 •
526 -
'•
568
1
17
35.29
0.80 •
0.022|
1
28.84
1
rt*\] f ...... •
-------
-95-
Location
Run Number
Primary Crusher
Conveyor Exhaust
,f ,« Gasket,:
WS y/5
Stack Pressure: P (in. Hg) = p. + p /13.6
* oar g
Stack Gas Velocity:
v$ (ft/sec) = 85.49 C (APT /P M }
r ^ «> S
1/2
Stack Gas Volume Flow Rate-
Qsd (dscf /min) = 1059 (1-BW A P /T
"•> S S S
Actual Stack Gas Volume Flow Rate-
Q (acf /min) = 60 v$ A
Weight of Paniculate Collected: m (mg )
3 /
Concentration of
Cs (gr/scf) = 0.01542 m /V (std)
C (g/dscm) = 0.03529 mn/Vm (std
n m v '
Mass Flow Rate of Particulate:
/»/-.•- •
- wi i ui w I V,U
Q (lb/hr) = 0.008571 C Q .
28.63
26.79
46.27
1350
1513
126.3
0.0585
28.73
26.71
48.77
1410
1590
192.4
0.0916
28.72
26.73
89.67
2590
2930
217.6
0.0697
28.71
26.79
32.67
1880
2100
2155.3
0.928
28.60
26.69
32.99
1850
28
26
32
18
2120
1626.8
0.701
11.1
20:
19
O.f
13
10
-------
Location:
Scrubber Inlet
Scrubber Outlet
Run Number:
Date:
Time Started:
Time Ended:
I
Barometric Pressure: P. (in. Hg.)
Static Pressure: P (in. O)
Area of Stack: A (ft2)
Pitot Coefficient: C
Meter Calibration- Factor: Y
Area of Nozzle: A (in )
Total Sampling Tine: "(Kin.)
Gas Sample Volume: Vm (ft )
Avg. Velocity Head: (V ap )?vg. (in. H20)
Avg. Orifice Pressure: AH (in H^O)
Avg. Stack Temperature: T (°R)
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica" Gel
Collected: VJc (ml.)
Gas Sample Volume @ Std. Cond.:
Vm(Std) (ft3) = 17.64 V-Y (?^ +AH/13.6)
Tm bar
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 Yj
Moisture Content: B f = : Vw(Std)
w" • Vm(Std) + Vw(Std)
Ftolecular Weight of Stack Gas (dry):
Kd = 0.44 (% C02) + 0.32 (% 02) +
0.28 (% N2+2 CO)
1
o
L.
3
11-13-79
0915
1030
27.16
-0.42
2.18
0.834
1.016
0.0302
56
43.117
1.0
1.65
.518
542
0
38.90
0.00
0.00
28.84
1340
1450
27.02
-0.42
2.18
0.834
1.016
0.0302
56
39.769
0.92
1.5
527
566
12
34.16
0.56
0.016
28.84
1715
1830
26.97
-0.42
2.18
0.834
1.016
0.0302
56
42.723
0.93
1.5
526
570
17
36.38
0.80
0.022
28.84
1
2
3
11-13-79
0904
1032
27.15
0.5
1.97
0.834
1.00
0.0269
78
60.875
1.4
1.8
523
532
15
55.069
0.71
0.013
28.84
1331
1454
27.02
0.5
1.97'
0.834
1.00
0.0269
78
59.996
1.3
1.7
527
547
14
52.52
0.66
0.012
28.34
1630
1816
26.97
0.5
1.97
0.834
1.00
0.0269
96
75.727
1.3
1.7
528
552
30
65.57
1.41
0.02]
28.8'
Scon Environmental Technology Inc
-------
-a/-
Location
Run Number
Molecular Weight of Stack Gas (wet):
Hs • «d (1-BWS) * 18.0 BW5
Stack Pressure: Pe (in. Hg) = P. + P/13.6
s oar 9
Stack Gas Velocity: 1/2
vs (ft/sec) = 85.49 Cp UPTS/PSMS)
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 (!-BWS)YS A PS/T$
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v A
Weight of Particulate Collected: m (mg.)
Concentration of Particulate @ Std.Cond.(dry)
Cc (gr/scf) = 0.01542 m /V (std)
C* (g/dscm) = 0.03529 mjj/vjj (std)
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.008571 C$ Q$d
Isokinetic Rate:
!<«• 13.61 TsVm(std)/PsvsAne(l-8ws)
Control Efficiency, % = ^in " Vit'
Q.
yin
Primary Crusher
Scrubber Inlet
1
28.84
27.13
58.01
7010
7590
265.0
0.105
6.3
103.0
2
28.66
26.99
56.44
6560
7380
700.8
0.316
17.8
96.7
3
28.61
26.94
56.81
6570
7430
557.6
0.236
13.3
102.8
Primary Crusher
Scrubber Outlet
1
28.70
27.19
69.06
7400
8160
38.8
0.0109
0.68
100.8
89.2
2
28.71
27.06
66.96
7080
7920
39.1
0.0115
0.69
100.3
96.1
3
8.61
7.01
7.20
020
7940
KJ.6
).009£
0.57
102.7
95.7
-------
Secondar
. Location: .93- ^
Run Humber:
Date:
Time Started:
Time Ended:
Barometric Pressure: P. (in. Hg.)
Static Pressure: P (in. HJ))
Area of Stack: A (ft2)
Pilot Coefficient: C
Meter Calibration -Factor: Y
2
Area of Nozzle: A (in )
n
Total Sampling Time: "(Min.)
Gas Sample Volume: Vm (ft3)
Avg. Velocity Head: (V~Zp )avg. (in. FLO)
Avg. Orifice Pressure: AH (in H^O)
Avg. Stack Temperature: T (°R)
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: V, (ml.)
Gas Sample Volume @ Std. Cond.:
Vm(Std) (ft3) = 17.64 VrnY (?k +AH/13.6)
Tm bar
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 YJc
Moisture Content: B = s Vw(Std)
Wj • Vm(Std) + Vw(Std)
tolecular Weight of Stack Gas (dry):
Kd = 0.44 (% C02) + 0.32 (% 02) +
0.28 (% \\fi CO)
4
11-14
1425
1607
26.25
-1.9
0.545
0.834"
1.00
0.0302
60
51.309
1.1
1.97
531
549
21
43.52
0.99
0.022
28.84
~y Crusher. Secondary Crus
ij
-------
-99-
Location
Run Number
Molecular Weight of Stack Gas (wet):
Hs a Hd C^HS' + 18'° Bws
Stack Pressure: P (in. Hg) = P. + P /13.6
s J bar g
Stack Gas Velocity: 1/2
vs (ft/sec) = 85.49 Cp UPT^M,.)
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 (!-BWS)YS A P$/TS
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v$ A
Weight of Particulate Collected: m (mg.)
Concentration of Particulate @ Std.Cond.(dry):
C_ (gr/scf) = 0.01542 m /V (std)
Cg (g/dscm) = 0.03529 m[[/vjj (std)
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.003571 C$ Q$(j
Isokinetic Rate:
M«- 13.61 T5Vm(std)/PsvsAne(l-Bws)
Secondary Crusher
Exhaust
4
28.60
26.11
63.06
1750
2060
5277.4
1.87
28.0
107.8
5
28.65
26.27
65.36
1850
2140
2389.7
0.820
13.0
105.5
6
28.58
25.27
65.56
1830
2140
2485.2
0.904
14.2
100.2
Secondary Crusher
Scrubber Inlet
4
28.70
25.44
52.05
8270
9810
1128.9
0.335
23.7
99.0
5
28.71
25.63
48.74
7880 .
9180
821.9
0.252
17.0
100.4
6
28.70
25.69
51.45
8250
9690
75.5.8
0.229
16.2
97.2
-------
Location:
Secondary Crusher
Scrubber Outlet
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: Pbgr (in. Hg.)
Static Pressure: P (in. O)
Area of Stack: A (ft2)
Pitot Coefficient: C
Meter Calibration- Factor: Y
o
Area of Nozzle: A (in )
Total Sampling Time: ^(Min.)
Gas Sample Volume: Vm (ft3)
Avg. Velocity Head: (VTp )avg. (in. O)
Avg. Orifice Pressure: AH (in H^O)
Avg. Stack Temperature: T (°R)
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: V]c (ml.)
Gas Sample Volume @ Std. Cond.:
Vm(Std) (ft3) = 17.64 VrnY (?^ +AH/13.6)
Tm bar
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 VJc
Moisture Content: B - s Yw(Std)
w" - Vm(Std) T Vw(Std)
Molecular Weight of Stack Gas (dry):
Hd = 0.44 (% C02) + 0.32 (% Og) +
0.28 (% N2+2 CO)
4
11-14
1525
1739
26.24
0.0
14.89
0.834
1.00
0.0585
96
67.282
0.23
1.57
524
556
23
56.26
1.08
0.019
28.84
5
11-15
0757
0956
26.38
0.0
14.89
0.834
1.00
0.0585
96
65.792
0.22
1.6
522
537
29
57.27
1.37
0.023
28.84
6
11-15
1100
1256
26.39
0.0
14.89
0.834
1.00
0.0585
96
6.095
0.22
1.6
525
559
30
55.29
1.41
0.025
28.84
.
•i
^cott Enwonmentev] lechnoJo^y Inc
-------
-1UJ.-
Location
Run Number
Molecular Weight of Stack Gas (wet):
Hs - Hd (1-BWS) + 18.0 Bws
Stack Pressure: P. {in. Hg) = P. , + P^/13.6
S Dor 9
Stack Gas Velocity: 1/2
v (ft/sec) = 85.49 C (APT /PM)
5 i p S S S
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 (l-Bws-)vs A P$/TS
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v A
Weight of Particulate Collected: m (mg.)
Concentration of Particulate @ Std.Cond.(dry):
C. (gr/scf) = 0.01542 m /V (std)
C* (g/dscm) = 0.03529 mjj/vjj (std)
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.008571 C$ Q$(J
Isokinetic Rate:
I (%) - 13.61 Ts Vm(std)/PsvsAn0(l-Bws)
Control Efficiency, % = ^Qin " Qout^100
^in
Secondary Crusher
^crubber Outlet
4
28.64
26.24 '
28.55
22100
25500
85.2
0.0234
4.4
97.2
81.4
5
28.59
26.38
27.82
21700
24900
43.0
0.0116
2.1
101.1
87.6
6
28.57
26.39
27.91
21600
24900
67.0
0.0187
3.5
98.0
78.4
t
i
-------
Location: -102-
Truck Loadout
Truck Loadout
Hood Exhaust
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: P. (in. Hg.)
Static Pressure: P (in. H?0)
Area of Stack: A (ft2)
Pi tot Coefficient: C
Meter Calibration- Factor: Y
2
Area of Nozzle: A (in )
Total Sampling Time: ^(Min.)
Gas Sample Volume: Vm (ft3)
Avg. Velocity Head: (V~7p )avg. (in. O)
Avg. Orifice Pressure: AH (in H?0)
Avg. Stack Temperature: T (°R)
*>
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: V]c (ml.)
Gas Sarr.ple Volume @ Std. Cond.:
Ym(Std) (ft3) = 17.64 VniY (Pk +AH/13.6)
Tm bQr
Volunie of -Water Vapor:
Vw (std) (ft3) = 0.04707 Vk
Moisture Content: B = : Vw(Std)
Wj - Vm(Std) + Vw(Std)
Molecular Weight of Stack Gas (dry):
Md = 0.44 (% C02) ••- 0.32 (% 0£) +
0.28 (% N2+Z CO)
7
11-16
1.155
"woT"""
26.31
-2.5
0.349
0.834
1.00
.0346
56
51.036
1.10
2.2 .
536
546
2
43.65
V
0.09
0.002
28.84
8
11-17
0800
1055
26.14
-2.5
0.349
0.834
1.00
0.0346
48
43.984
1.2
2.4
522
527
18
38.74
0.85
0.021
28.84
9
11-17
1203
1450
26.03
-2.5
0.349
0.834
1.00
0.0346
48
42.705
1.1
2.26
528
532
9
37.09
0.42
0.011
28.84
7
11-16
1155
1405
26.31
-0.95
0.518
0.834
1.00 .
0.0346
60
51.69
0.91
1.9
533
543
4
44.41
0.19
0.004
28.84
8
11-17,
0800
1100
26.14
-0.95
0.518
0.834
1.00
0.0346
60
53,075
0.96
2.0
519
528
12
46.61
0.56
0.012
28.84
9 '
fcjsmctay** mm.'
11-17
1200
ror
26..03,
-0.95
0.518
0.834
1.00
.0346
60
1.76
0.92
1.9
526
534
5
44.75
0.24
O.OOE
28.8'
IWI ^cotr Environmental Techncto^y Inc
-------
-103-
Location
Run Number
tolecular Weight of Stack Gas (wet):
"s * Md d^ + 18'° B«s
Stack Pressure: Pc (in. Hg) = P. + P 713.6
s oar g
Stack Gas Velocity: 1/2
vs (ft/sec) = 85.49 Cp UPyP^)
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 (!-BWS)VS A P$/TS
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v A
Weight of Particulate Collected: m (mg.)
Concentration of Particulate @ Std.Cond.(dry)
C. (gr/scf) = 0.01542 m n/V (std)
C^ (g/dscm) = 0.03529 mjj/vjj (std)
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.003571 C$ Q$d
Isokinetic Rate:
K«- 13.61 TsVm(std)/PsvsAne(l-Bws)
Truck Loadout
Conveyor Exhaust
7
8.82
6.13
63.10
1130
1320
1709.5
0.604
5.9
39.9
8
28.61
25.96
65.49
1180
1370
1234.0
0.491
5.0
99.6
. 9
28.72
25.85
63.07
1130
1320
2413.4
1.00
9.7
99.6
Truck Loadout
Hood Exhaust
i
28.79
26.24
57.13
1540
1780
160.1
0.0556
0.73
104.0
8
28.71
26.07
58,17
1580
1810
87.2
0.0288
0.39
105.8
9
8.78
5.96
7.38
550
780
28.3
i.
)098
).12
104.1
-------
Location:
Truck Loadout
Fxhaust
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: Pbar (in. Hg.)
Static Pressure: P (in. H.O)
Area of Stack: A (ft2)
Pitot Coefficient: C
Meter Calibration- Factor: Y
2
Area of Nozzle: A (in )
Total Sampling Time: ^(Min.)
Gas Sample Volume: Vm (ft3)
Avg. Velocity Head: (V^Zp )avg. (in. H^O)
Avg. Orifice Pressure: AH (in H?0)
Avg. Stack Temperature: T (°R)
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica" Gel
Collected: V. (ml.)
lc
Gas Sample Volume 0 Std. Cond.:
Ym(Std) (ft3) = 17.64 VrnY (?u +AH/13.6)
Tm bar
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 Vj
Foisture Content: B = : Vw(Std)
^ • Vm(Std) + Vw(Std)
Molecular Weight of Stack Gas (dry):
Hd = 0.44 (% C02) + 0.32 (% 02) +
0.28 (35 N2+2 CO)
(\) Scott Environmental Techrotor/ inc
7
11-16
1200
1414
26.31
0.0
0.914
0.834
1.00
0.0302
56
39.052
0.80
1.36
540
539
,4
33 7^
OO. / 3
0.19
0.006
28.84
8
1-17
0804
1101
26.14
0.0
0.914
0.834
1.00
0.0302
54.58
39.357
0.90
1.5
522
523
14
34 R^
0.66
0.019
28.84
9
11-17
1203
1546
26.06
0.0
0.914
0.834
1.00
0.0302
56
38.937
0.82
1.4
532 '
530
9
33 Q1
00 . y i
0.42
0.012
28.84
.
-
-------
-105-
Location
Run Number
Molecular Weight of Stack Gas (wet):
Hr a M. (1-B J + 18.0 B
s d x ws' ws
Stack Pressure: Pc (in. Hg) = P. + Pn/13.6
s uar 9
Stack Gas Velocity: 1/2
v (ft/sec) = 85.49 C (APT /PH.)
s p s s s
Stack Gas Volume Flow Rate:
Q . (dscf /min) = 1059 (1-B • )v A P /T
.so . ws s s s
Actual Stack Gas Volume Flow Rate:
Q (acf /nrin) = 60 vg A
Weight of Participate Collected: m (mg.)
Concentration of Particulate @ Std.Cond.(dry):
Cc (gr/scf) = 0.01542 m /V (std)
C* fg/dscm) = 0.03529 n/j/VjJ (std)
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.008571 C$ Q$(j
Isokinetic Rate:
I (55) = 13.61 Ts Vm(std)/P$vsAn9(l-Bws
Control Efficiency, % = ^Qin " Qout^100
Qin
Truck Loadout
Baghouse Exhaust
I
7
28.78
26.31
53.85
2530
2950
19.2
0.0088
0.18
104.1
97.2
8
28.64
26.14
56.48
-
2690
3100
35.8
0.0158
0.36
103.6
93.7
9-
28.71
26.06
54.45
2550
2990
33.6
0.0153
0.33
103.6
96.6
-------
#2701-01-0280 -106-
APPENDIX B
PARTICULATE FIELD DATA SHEETS
Scott Environmental Technology Inc.
-------
PROJECT NUMEER
TEST NUMBER
FIELD DATA SHEL7
-107-
PLANT f', /.:',.., /,. ,.-. ••>,*'. > v-
DATE
PR03E LENGTH & TYPE r-J > *..t, 'u-i^.j
NOZZLE I.D.
SCOn ENVI9ONMENTAL TECHNOLOGY. INC.
FYRITE ANALYSIS
SAMPLING LOCATION y;'-,,-j- v..'.-^ t'..rf. yi -,,,^ 7 SAMPLE BOX NUK2ER & . ..^'-':.. '-'~
SAMPLE TYPE ^>•,-?>„/ :; METER BOX NUMBER & J . ^ '<<
RUN NUMBER if' ?, -. ' r i PROSE HEATER SETTING -
OPERATORS \'. <* - ^ FILTER HEATER SETTING •/.',-'
AMBIENT TEMPERATURE -•''" ^ REFERENCE iP '"' ~
BAROMETER
co2 o2
READ AND RECORD ALL DATA EVERY •", MINUTES PITOT NUMBER
-'•••••• •' ...,-• y^.-f-h^.Ct^t.r.ies,
TRAVERSE
KUY8M
/
4
J
(/
5
(,
i
•A
•-5
o'
.-
/,•
CL
SA,T?LM
TlVE.c.a
0
__
U
lr;
.;
^ —
.f-
f-
jj
/-'
OCX USE
CLOCK!
*",<.# "'"
IMTIAL: '• • '•• -
.'. i°.-.^- '
•'. , • • !
| -
1
• 4. ^" /
J.
• • > ' ' ^' ' )
'.•'• '1. ' •••' -}_
:•-.• /
"-.-.v-i- - '•• /
^ 1
.J"
v'-
:•'
/'. -,-'--> i
r r.
V
^ X -j n ;—
VELOCITY
HEAD
.-. .f
. "}•'
-'-
CRlfiCE PRESSURE
OIFFERJ.1TIAL
li.1). it. h,0]
OESiRi:
/./'
/55
SCTWL
l./f
/.5$
/,^ /rSi
«?3
/ . / !c3 3
/..'
-,.•
. ^ '>
/. .
/. /
-' .-
; i
0.^
J 3
A "'5
/r-5
.-J?. 3
P. 3
=3.V
^..3
-< '"I
S3
3,'-}
/.'-'S
//•3
-0.3
•P-3
-7//
•^.5
i.°
STACS
TEy?ERATUSE
(T.I.'F
67
67
• ^,5
('t
.?3
\.'f j
'
CUTLET
'T=K.'-'f
7'J*J'A'3'>.n<\J!ffi &«•<•
(/
•)fi\
•lo
Iff
sc
SO
-••''/
• -7 ">
S'3
&6:
E.O 7~.
. . f f
\, "V/>- ' ' / " / -- ,"f~ /• f J *
4,
TaWHSE
?J..1T
.VJV3£S
Cl
Si.vrL:h:
TiV£.M.i
:* THE
Cl l»
CLOCXI
i
CSSJfETlRREAClnG
iv,i. r^
I
VELCCITY
HEID
l»,l. ia. KjO
CIIFiCEPRE'.SURE
HFFE'E.liML
OtSiRED
ACTUAL
su;<
TE;;?t.:iJTa!£
a,i.-F
curcy VETER
TEIT.'ERITUF.E
-
PU'J."
••ACUIK.
' IT. l-.|
1
l«>:s:£
ItiKPEEAT
"F
t'REJ
CCMI'ENTS
-------
NOMOGRAPH DATA BY
MOISTURE
W.PINGERS
FINAL VOLUME
INITIAL VOLUME
KET VOLUV.E
ANALYTICAL DATA BY
SILICA ca
FINAL WEIGHT 2
INITIAL WEIGHT c
NET WEIGHT .
TOTAL KOISTURE
'*-- . I
^H^Li
iVf t
i>
-108-
&-3:3~
I
ACETONE FRONT WASH
FINAL r?f If.Kfr
TARE rQ.02.2^
NET ? b.C '
FILTER NUMBER 1
FINAL -a L-IS>
TARE 7.3,T~
NET 1,1 '
FILTER NUMBER ?.
FINAL
TARE
NET
FILTER NUMBER 3
FINAL '
TARE
NET
CYCLONE
FINAL
TARE
NET
mg
mg
mg
ACETONE BACK WASH
FINAL
TARE
NET
ng
ing
mg
ETHER-CHLOROFORM EXTRACT
mg
mg
mg
mg
mg
mg
mg
mg
mg
mq
mg
. mg
FINAL
TARE
NET
WATER EVAPORATION
FINAL
TARE
NET
TOTAL BACK
mg
mg
mg
mg
mg
mg
mg
I CERTIFY THAT THt SA.rPt.ES DESC'lEE!:
BY THIS KTA SHEE" WESE CCiLECTiD IS
a:CCRQS.'iCE 'JITH HEThO^S CL'TLiSED BY
UEP.E :« Tn- POSSESSION of.
FOB SHIF-Eh7 BY COK^i CAP
KYSELr U.MIL DELIVERY TO A
F0« ANALYSIS.
SIGNED
WITNESS
i cE»iirY TH;T i SEC-lV't'
W SEALCC
Bit? SS.
LA60»ATORY
OAT-
WT-:
THE SS-:LES
TOTAL FRONT ?7.I
mg
.
• SOVE SS'SO IKf.lvJK.*. Ai:o »s:.Y2ED
THE" IN ACCORDANCE '.'ITh THr AKOt-
1A.1ED PROCEDURE.
CALIBRATED PRESSURE CirFESEHTiAl A»OSS
ORIFICE, m. .4.0
AVER ACE PETER TEl'»ERATURE(A'> STREW BV VQLUV.E
BAROSE7RIC PBE'S!«E ST VETER. it. HI
STATIC PF.ESSJRE IS !t«CK. n. K|
P,i^.n i STACKCf.UCE PRESSURE e. ,». H;o)
RATIO OF STATIC PRESSURE TO *ETER PRESSURE
AVEP.1GE HACK TE."?ERATUR=. °f
AVERA:E VELOCITY «A:. m. d,o
KMKlNI VELOCITY «EAO. in. H;0
c FACTC*
CALCULATES NOZ2LE OUVETER. in.
ACTUAL BGriLE DUVET ER. «.
REFERENCE it, in. tijO -
iK,
T'»t
^,
%
',
'•-.
TV«.
".n
*»«,.
DRY MOLECULAR WEIGHT DETERMINATION BY
SAMPLING TI.VE (24-hi CLOCK)
SAMPLING LOCATION
SAAiPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL KETHOD
AY.BIENT TEKPERATURE__
RtAOinc Rirria HCTUAL
COiNfTtidCTUALCa
RttDir:ciiNLCnau*-
Oj R
WITHESS
;s §
.
O Z
-2
> to to ^«
O IS)
' CC. Ul
CUO
I
lei
Er -"M
"S'l
s
2=
Si ~
-------
PROJECT NUMBER " ' TEST NUMBER *r
PLANT C.V
/ "1
FIELD DATA SHEET
09-
3E LENGTH & TYPE 1* ,' ,i_ A •..*,
&f' DATE n||4.'llV NOZZLE I
i5?. '/ .
$£• -- -
D.
<$
SCOn INVIBONMENTAt tfCNNOLOCY. IMC.
. \°>&
FYRITE ANALYSIS
CO, 0,
SAMPLING LOCATION r^to^-oatiVieu.-su, ^x-uWsf SAMPLE BOX NUMBER C'V'-vT PP. =»v\.i-r ^l_
SAMPLE TYPE
iv\F?-mcro •? METER BOX NUMBER •'.vii ^--." ^n- 'I.M
RUN NUMBER 4— PROSE HEATER SETTING ,)/.v-
OPERATORS <"•£. FILTER HEATER SETTING \\ -'A-
< . AMBIENT TEMPERATURE f,|/f' f? /^tJ* REFERENCE iP l.oC
•-"-. BAROMETER t
v
* s •
; ;'',/'•
"*•,••
7.<-. .
V':f ~ " .-"•
S'"'.- . •
r-:77-- :
-'V- ••
IH
i '. *•'.:•£
' ?*i;+3&*-f=r&*
*$i£-'~
l
V-
(V
1
1
f
-
\
J
'
:*.""
1
1
I
i
>
»
j
i
TRAVERSE
POJT
BUYEER
1
r
3
4
£
• t>
T
f,
9
15
H
— }1.
(s.l'Z _P 14-tnj READ AND RECORD ALL DATA EVERY -^MINUTES
CLC
SA.«PLIKC
Tll'i.tm
^
0
,<
?A
a<
l-o
-jf
/,/!•
../s'
O
^<
— ItO
CK TIM
121 bi
CLOCK)
CA! f.CTER READm:
INITIAL: 4-no.-7?.n
•4 T3,, SI'S"
4T«).C"!xC
4- 9 1* .r cro
A 8 (r . {-• L. "I
• 4ei .^fti
,"'Mr 49fr. IT-4-
493 —
^05., Sl<
-=• ^t>p. 1 1, 1
^n^. 41,9
•5IT. ^o|
7¥'
VELOCITY
HEAD
Up,), b. H jO
,ft"?
£,<
.or
i •?>"
i.-j,
1,3 .
.10
I o<
I, of
|,0<
\'"j
I. ^
/
I.I'
4, r.v-.-.oji, i.|
ORIFICE PRESSURE
OlFFERENTHL
UM). in. HjO)
JES.'REO
.$T
l.*^
,%^
l.t
^.•5
T.3
.11
,9?"
l,»^
\-t><
1.*
1>-?>
*
ACTUAl.
1-^1
.&z
.?-;
?. .7^
~i.*>
i:$
1,11
!,^
1,8*
/.•}$
2.^
^-.5
•^'1
STACK
TEXPERATURE
(T,l. F
">V
11
IV
n-u
it-
H
11
11
1i
1\
-11
y
DRVCU BETED
TW7ERATURE
INLET
-J2,
-n
es
93
icni
(£,(,
fit
^0
Q-]
\0^
110
|I6>
OUTLET
1^
")*>
-?C.
16
«l
8^"
&t>
6S
?fr
;3o
^3
^
PUSP
VACUU*.
\0<
n-*
\1.o
>C.o
\r.»
1 .t.
-9.0
ll.o
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/a'*
iC.o
i^.»
^T
tyA
IKPINCE
EMPERATl
• "F
^p
^T^
•>>
"Tb
*T1>
-."»
?T>
5D
5T>
-5b
PITOTMIMBFR
REJ
COMMENTS
'.^V/ ietL^-nt^r"
•— ' ^_
1 ' ' ii
•^^^•^~' ~^^»"— ^-"-^- — 1*^.'— ~— — -—**»"••--•-: S=--7-> .' ---— - -v— - '- •-' ^" ;;.•> <~ -- — »: — a.^K»— .7. -.' --••.' »^'
TRMESSE
CL
SAXTLINS
t
1CK T^E
CLOCKI
CAiKEIER READING
IV.I. It'
,
1
)
i
I
< *
VELOCITY
HEAD
(&9t). in. K^O
.
CSIFICE F
QIFFEa
DES'.REO
RESWHE
ACTUAL
STACK
rr.i.-F
TEKPERA1USE
IKLET
OUTLEL,
PUV.P
VACUUM.
«. Hi
HtPl.lCE
EBPERAT
"F
R
URE.
COMMENTS
•
-------
f*
MOISTURE
HPINGERS
FINAL VOLUME - /-I0-6 nl
INITIAL VOLUME _Cr2_» rjl
NET VOLUME
-110-
NOMOGRAPK DATA BY
JIUCAGEL
FINAL WEIGHT
INITIAL WEIGHT
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MOISTURE
-116-
NOMOGRAPH DATA BY
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FINAL VOLUffi
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I CERTIFY THAT THE EMPLES DESCRIBED
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PROJECT NUMBER mi
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MOISTURE
KPIN2ERS
FINAL VOLUME ^00
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MOISTURE
KPINGERS
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INITIAL VOLUME.
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MOISTURE
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NOMOGRAPH DATA BY
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NOMOGRAPH DATA BY
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FINAL TOGHT f-" \-5 (
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I CERTIFY THAT THE SABLES DESCRIBED
BY THIS DATA SHEET WERE COLLECTED IN
ACCORDANCE WITH HETKSS OUTLINED B<
WERE IN THE POSSESSION S, OR S-AIED
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-128- NOMOGRAPH DATA
MOISTURE
WINGERS
FINAL VOLUSE
INITIAL VOLUME ?'e~° '_•
NET VOLUME .''
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SILICA GEL ,/_,
FINAL HEIGHT " ~' ;- '-• |
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ANALYTICAL DATA BY
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mg
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mg
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ACETONE BACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM FXTRACT
FINAL mg
TARE mg
NET mg
WATER EVAPORATION
FINAL ' mg
TARE mg
NET mg
TOTAL BACK mg
1 CERTIFY TH»T THE SAHPIES OESCP1BEO
BY THIS DATA SHEET W-SE COLLECTED IN
ACCORDANCE WITH METHODS OUTLINE:- BY
Wt«£ I» THE POS!ESSiCI Of. 0» SEALED
FOR SliiP.XENT 51 CCrt^sl CARRIER 3Y,
HYSELf UiTil OCLIVEai TO A LABOMTORY
FOR AML'SIS.
SICHEO DATE
WITNESS MTE
I CEDTIFY TWT r SECEfVrBTHE SH^fTlTS
CALIBRATES PRESSURE DiFFEBEKT!«. ACROSS
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ANALYTICAL METHOD
AMBIENT TEMPERATURE
TOTAL FRONT
DESCRIBED BY THIS KTA SHEET FfiOH THE
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-129-
PROJECT NUMBER mu( TEST NUMBER
PLANT ftVp^ci^-'' 3Fvt>.&"3i ^li^vv-- Co
DATE nl i^-H-i
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RUN NUMBER '.'_.
OPERATORS -T.^. / i-'-. ,;\ ,
AMBIENT TEMPERATURE po"''&. 13,30
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PROSE LENGTH i TYPE 'i'
NOZZLE 1.0. . i-^io
SAMPLE BOX NUMBER '.'•>?<"
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-130- NOMOGRAPH DATA BY
MOISTURE
MPINGERS
FINAL VOLUME
INITIAL VCLUVE
RET VOLUME
l£
1,Cr
f-°
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nl
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FINAL HEIGHT
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ANALYTICAL DATA BY
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ETHER-CHLOROFORM EXTRACT
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WATER EVAPORATION
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TOTAL BACK mg
I CERTIFY THAT THE SAMPLES DESCRIBED
BY THIS OAK SniET '.ERE COLLECTED III
ACCORDANCE UlfH METHODS OUTLINED BY
HERE IN THE'POHESSIW OF. OR SEALED
MYSELF UNTIL 90.1VCRV TO A L«80«TCB»
FOR AXSLTSIS.
SIGNED OATE
WITNESS OATE
I CERTIFY fKlf! RttEIVUn'HE SAnTCfS
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SAMPLING LOCATION
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ANALYTICAL METHOD
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SCOn ENVIRONMENTAL TECHNOLOGY, INC
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PROJECT NUMBER
PLANT
DATE 1 1 1 1 "-> 1 1 3
-131-
TEST NUMBER FIELD DATA SHEET
PROBE LENGTH I, TYPE
NOZZLE I.D.
VItONMCNTAL TECHNOLOGY. IMC
SAMPLING LOCATION ?/c^
SAMPLE TYPE lUCTVlfp ^
RUN NUMBER *>
OPERATORS T*i> / g- ^
FYRITE ANALYSIS
CO, 0, _
SAMPLE BOX NUMBER
METER BOX NUMBER
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AMBIENT TEMPERATURE
BAROMETER -7.
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FILTER HEATER SETTING
REFERENCE &P \.\t
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READ AND RECORD ALL DATA EVERY
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"COMMENTS
-------
-132- NOMOGRAPH DATA BY
JjOISTURE
BIPINGERS
FINAL VOLUffi I*
INITIAL VOLUME *•
HET VOLUME —
*^'° ml
"°-° ml
3.° r.l
SIUCA UcL
FINAL HEIGHT
INITIAL WEIGHT
NET WEIGHT .
TOTAL MOISTURE
£73.3 t
_ll£5l
. 7-f i
0
ANALYTICAL DATA BY
ACETONE FRONT WASH
FINALR-),-?2.!oS
TARE SI. 10 1.4-
NET . $ I 1 - 1 '
FILTER NUMBER 1
FINAL . 40S.f
TARE . If!-" ,
NET 315'
FILTER NUMBER 2
FINAL
TARE
NET
FJLTER NUMBER 3
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
ACETONE SACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE rng
NET mg
WATER EVAPORATION
FINAL • mg
TARE mg
NET ' mg
TOTAL BACK mg
I CERTIFY THAT THE SWPLES OE5C<*:BED
BY THIS D*TA SHEET WERE COLLECTED IN
ACCORDANCE WITH HTHCOS OUTLINED BY
WERE IN THE POSSESSION OF, OR SEALED
FOR SHIPMENT Bf COWOK CARRIER BY.
KYSELF UNTIL DELIVERY TO A LABORATORY
fO« ANALYSIS.
SIGNED DATE
HITNESS OATI
I tlKTIrY THAT I SECHvEE) T.rE SW>LFS
TOTAL FRONT
_mg .
DESC3I3ED BY THIS WTA SHEET ?BO« THE
ABOVE HA.XED INDIVIWAL A.10 ANALYZED
THEB IS ACCCROAWE aiTH THE ABOVE
KAMEO P«OCEOU«£.
VIRONMENTAL TECHNOLOGY. INC.
SIGNED
DATE
-T^it; "r'\
Zh:i:tr:.::H.~-
^rzrir^lt:
... ..I ..._—.-—^.'••-•••
;--: .'curt: ;rz::"~
CALIBRATED PRESSURt DIFFESEIITIAt. ACROSS
ORIFICE. h.HjO
AVERAGE rETERTEKPERArUREIASeiEN^n'Fl.'F
PERCENT WISTUBE IB CAS STREAS 8Y VOL1OE
BAROBErRIC PRESSURE AT BF.TES. l«. H|
STATIC PRESSURE IN STACK, in. H|
P.i^.Ul i HACK CAUCE PRESSURE in in. H2o)
RATIO OF STATIC PRESSURE TO UETER PRESSURE
AVERAGE STACK TEMPERATURE, 'f
AVERAGE VELOCnr HEAD, in. «,0
KAXIMI VELOCITY HEAD. in. ttf
C FACTOR
CALCULATED NOZZLE NATTER, in.
ACTUAL NOZZLE DIMETER, in.
REFERENCE ij. i». K;0
4H,
T'-l-
«« .
%
',
"'/P.
V
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«»«..
DRY MOLECULAR WEIGHT DETERMINATION
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
AMBIENT TEMPERATURE
~^\_^ RUN
GAS ^^
C02
021NET K ACTUAL Oj
R£«CinG!lH1JS ACTUAL
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COlHET IS ACTUAL CO
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1
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KMtHC
nn
AVERAGE
MET
VOLlffiE
-------
PROJECT NUMBER 3-7 o
PLANT Cvyp^^xo O
DATE Ij) !///£
> . SAMPLING LOCATION' Mvc_
'' SAMPLE TYPE I^JiidL*
RUN NUMBER I
OPERATORS 3~Uy -
AMBIENT TEMPERATURE
f TEST NUMBER -1
C^flv<^«-
6.3
xor
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60
till
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10
11
-------
-134- NOMOGRAPH DATA BY
WINGERS
FINAL VOLUKE
WITIAL VOLUME
NET VOLUME
ANALYTICAL DATA BY
ACETONE FRONT WASH
FINAL 1
TARE
NET
SILICA GEL
FINAL WEIGHT
INITIAL KEIGHT
KET WEIGHT
TOTAL MOISTURE
I f /T
J*
_mg
_mg
ACETONE BACK WASH
FINAL
TARE
NET
_mg
_mg
jng
FILTER NUMBER 1
FINAL .3"7?r
NET
FILTER NUMBER 2
~
jng
jng
_mg .,
mg
TARE ^
NET ^ "
FILTER NUMBER 3
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET
mg
mg
mg
mg
mg
mg
mg
mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
-NET mg
WATER EVAPORATION
FINAL mg
TARE mg
NET mg
TOTAL BACK mg
CALISSATEO PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. HjO
1
AVERASc Kin rEXPERATURE (MJJE«T»a'F).'F
PERCE.NT r.tKTjP.t INCUS STREWS EY VOLLW£
SAR«IF.TRiC PRESSURE AT KETER. in. «j
STATIC PRESSURE IS STACK, in. H|
P.i^.CU > STACK GAUGE PRESSURE a in. H2o)
RATIO OF STATIC P8E5SUSE TO METER PRESSURE
AVERAGE SfACK TEMPERATURE. «F
AVERAGE VELOCITY HEAD. in. Hf
tUlKiit VELOCITY H£AO. i«. HjO
C FACTOR
CALCULATE.1) NDULC DIAVETER. in.
ACTUAL KOIZLE OlAXETEfl, a.
REFERENCE ij. in. H,0
4K,
T'^
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£>c?
I-3-7
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DRY MOLECULAR WEIGHT DETERMINATION
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION
BY
I CEBTIfY THAT THE SAMPLES OESCHIBEO
BY THIS DATA SHEET UE3E COLLECTED IK
ACCOfiMflCE WITH METHCOS OUTLINED BY
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
AMBIENT TEMPERATURE
I FATHER CERTIFY THAT TH- SAMPLES
MERE IN THE POSSESSION CT, 03 SEALED
FOR SHIPNEUT BY CCWON CARRIER 3>.
KYSELF U.1TIL DELIVERY TO A LABORATORY
FOR AKALYSIS.
DATE
TOTAL FRONT
_mg.
SIGNED
UIThESS DATE
1 CESTIfY VuAT rHKEIvED TKE SASflTs
DESCRIBED BY THIS DATA SHEET F33B THE
A50VE .WED INDIVIDUAL A«D AMLYIEO
THEM IN ACCW3ANCE WITH THE ABOVE
NAMED PROCEDURE.
[^~N. RUN
CAS ^N^
C02
RE.\DI.1G P.iHUS ACTUAi.
CO; REJlOlfiC)
COjNET n ACTJALCO
fitM)ir,Gti-»Lri ACTUAL
ACTUAL CO ft£AO»Q
1
RE A3 WC
^
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ACTUAL
REACIhC
HET
1
ACTUAL
an
AVERAGE
RET
VW.WEE
-------
PROJECT NUMBER Z>o ( TEST NUMBER ~135TIELD DATA SHEET
PLANT
DATE
SAMPLING LOCATION
SAMPLE TYPE S"
RUN NUMBER "2—
t^~~/
J
OPERATORS *-0
f}
READ AND RECORD ALL DATA EVERY
JNVHONMtNIAl TECHNOLOGY, IM
FYRITE ANALYSIS
CO, 0, _
MINUTES PITOT NUMBER.
TRAVERSE
P0..1T
BIBBER
CLOCK TUE
IAYPLING (M ki
TU'.£.««i CLOCK)
GJU rETER BEAPIBS
IHITIAL:
VELOClTIf
HEW
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DESIRED
ORIFICE PRESSURE
DIFFERt(IIl«L
(ill. i«. HjO)
ACTUAL
STACK
TE«?ER»TURE
DRfCUttTER
TEJtfERATURE
IM.ET
OUTLET
(T.Kt).'F
VACUU1.
in. H|
IWISCER
EWERATUREj
•F
COMMENTS
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61
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70
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60
CAS.-.EHRRLADI.IG
6 5"7,
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ORIFICE PRESSURE
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Ill
(0
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-------
-136-
JOISTURE
HPINGERS
FINAL VOLUME
WITIAL VOLUME
KET VOLUME
SILICA GEL
FINAL WEIGHT 2-flO.JL. I
'HITIAL KFIfiHT gtoto-^- t
NET WEIGHT _LL-~L_ t
TOTAL MOISTURE H
ANALYTICAL DATA BY _
ACETONE FRONT WASH
FINAL g*T. gCTZ- ng
TARE ft4T.fi 33.2. / mg
NET ' Ik- 0
?,£-
FILTER NUMBER 1
FINAL
TARE
.1
FLTER NUMBER 2
TOTAL FRONT
mg
jng
jng
jng
FINAL ^
TARE
NET
FILTER NUMBER 3
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET
•^9 mg
mg
mg
mg
mg
mg
mg
mg
mg
_n>9
ACETONE BACK WASH
FINAL
TARE
NET
ETHER-CHLOROFORM
FINAL
TARE
NET
WATER EVAPORATION
FINAL
TARE
NET
TOTAL BACK
mg
mg
mg
EXTRACT
mg
mg
mg
mq
mg
mg
mg
1 CERTIFY T:iAT THE SMPLES DESCRIBED
BY THIS OAfA SHEET WESE COLLECTED IN
ACCCRCANCE WITH KETHCOS OUTLINED Br
I FURrtfS iESTIfV ThA"; tHE
WERE IN IKE POSSESSION OF. OS SEA'.ED
FOR SHIPMENT 3i CO^^*>J CA?1IER 5T.
"YSELF U1TIL OELIVEiif 10 A LABOMTORJ
FOR ANALYSIS.
SIGNED
WITNESS
_OA7E_
DATE
DESCRIBED BT THIS GfiTA SHEET FROM THE
ABOVE SANED l»(i;»I»JJi. AND ASALYZED
THEM IN ACCORDANCE WITH THE ABOVE
KAKED FHOCEOUSE.
SCOn ENVIRONMENTAL TECHNOLOGY, INC.
SIGNED
_OATE_
DA IE
NOMOGRAPH DATA BY
CALIBRATES PRES1URE OlFFDIESTiU. »CROSS
OftlFlCe. k. HjO
AVERACE KETER TEKPERATuBE !A*i
° .
a — .
to
2:
STACK GAUGE PRESSURE 1n. H?0 -v^~
NEAREST UPSTREAM DISTURBANCE
NEAREST DOWNSTREAM DISTURBANCE!
PROCESS & CONTROL EQUIPMENT
DESCRIPTION
(C
ij
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Ik .
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PROJECT NUMBER .
PLANT CM/VVI^
DATE «?,/„/>
SAMPLING LOCATION '
SAMPLE TYPE *>""
RUN NUMBER Qfff=^
7-70 f
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4.
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TEST NUMBER ~1-
uJ
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S
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PROBE LENGTH S TYPE -f&"f *v^"o
NOZZLE I.D. ./.^5~
SAMPLE BOX NUMBER /? A^- t-
METER BOX NUMBER /? A-C. X
PROBE HEATER SETTING ?.
1, 1
? 7
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18
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ORIFICE FRESSJK
OlFfESr.MUL
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STACK
EMPERATURE
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TEK-ERATURE
miFT | n'lTitT
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-------
-138- NOMOGRAPH DATA BY
MOISTURE
WRINGERS
FIHALVOLIKSE 3-1 &- cl
WITIAL VOLUME JL'£2_ T.I
HET VOLUME /,$• ir.l
ANALYTICAL DATA BY
SILICA GEL
FINAL HEIGHT
INITIAL WEIGHT
NET WEIGHT
TOTAL MOISTURE
2 Sfe S
ACETONE FRONT VIASH
FINAL /O^ASDhT-
TARE /OJb.'V-S 1. i
NET 1$. \
FILTER NUMBER 1
FINAL . STqs-
TARE^.'Sb^-O
NET' (S.if '
FILTER NUMBER 2
FINAL
TARE
NET
FILTER NUMBER 3
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET
mg
mg
' mg
mg
mg j
mg/
^
mg
mg
mg
mg
mg
mg
mg
mg
ACETONE BACK HASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
' TARE mg
NET mg
WATER EVAPORATION
FINAL . mg
TARE mg
NET mg
TOTAL BACK mg
1 CERTIFY THAT THE SAMPLES DESCRIBES
8Y THIS DATA SHEET WERE COLlECrED IN
ACCORDANCE W1T» HETr!0£>S OUTLINED BY
HERE in TSE POSSESSION Of, K SEALED
FOR SHIPMENT BY COMMON CAFRIER S»,
MYSELF UNTIL DELIVERY TO A LA60PJ>TCRY
FOR ANALYSIS.
SIGNED OATE
WITNESS OATE
I CEITlfV TiAt' 1 DECEIVED tHE SMflES
TOTAL FRONT
_mg
CNVIRONMCNT4.L TeCHNOlOGY. INC.
CESCBISEO 3r THIS DATA SHEET FROM THE
ABOVE \JWEO I.'»
'.
'•
''/P.
Tw
",„.
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DRY MOLECULAR WEIGHT DETERMINATION BY
SAMPLING TIME (21-hr CLOCK)
SAMPLING LOCATION
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
AMBIENT TEMPERATURE
^"^V. RUN
CAS ^^\
C02
OjiSET IS ACTUAL 0^
RtAOtHC KI.1US ACTUAL
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CO;fi£TIJ ACTUAL CO
R£*mKC tlSUJ ACTUAL
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PROJECT NUMBER ")• Til TEST NUMBER H
PLANT 6U.,
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M. fl>e^.J'.fJ PROBE LENGTH &
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TYPE V/^-t^^.-^
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SAMPLING LOCATION Aa^w-^v, (/v*,»/.t>v* - .. SAMPLE BOX NUMBER jiU •'•£ £•*•/- * 2
SAMPLE TYPE
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TRAVERSE
PO:.1T
IMMBEJt
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COMMENTS
-------
-140- NOMOGRAPH DATA BY
MOISTURE
WRINGERS
FI.1AL VOLUME
INITIAL VOLUME
HET VOLUME
ANALYTICAL DATA BY
SILICA GEL
FINAL WEIGHT
INITIAL KEiGKl
NET WEIGHT
TOTAL KOISTURE
J2 t & 2 .
ACETONE FRONT
FINAL 92.1^
TARE qi.Ob
NET | 0?
FILTER NUMBER
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FINAL
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FILTER HUHBie.
FINAL
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NET
CYCLONE
FINAL
TARE
NET
TOTAL FRONT,'
X
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1 fc€> mg
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mg
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mg
mg
mg
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ACETONF BACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NF.T mg
WATER EVAPORATION
FINAL . mg
TARE mg
NET mg
TOTAL BACK mg
I CERTIFY THAT THE SAMPLES DESCRIBED
8Y THIS DATA SHEE! «SE COILECIEC IS
ACCORDANCE W!ra KETXCOS OUTLINED BY
WERE IN THE POSSESSION Of" OR SULEO
FOR SHIPMENT ST CCW3.1 CARRIER 2Y,
HY5EI.F UMI1L CELIVERY 10 A LABOPATORY
FOR AMLYSIS.
SI6»EO OATE
WITNESS DATE
I ctRiin THAV ! RicEivtO T« SA.*LES
\ DCSCRIBEO EY 7MS JATA ShtET T3>1 HiE
ABOVE NWED IhRIVIDCAL AND ANALfZED
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MA1EO PROCEDURE .
SIGNED OATE
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CALIBSAIED PRESSURE DIFFERENTIAL «CSO!S
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•VERAGEIIETER TEMPERATURE (MBIENTtJl'Fl.'F
PERCEliT KOISTURE III C*5 STREW Br »OLIK£
BAROMETRIC PRESSME AT KETER. in. K|
STATIC PRESSURE IS STACK, in. H|
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RATIOOf STAIIC PRESSURE TO «ETER PRESSURE
AVERAGE STACK TEMPERATURE, *F
AVERAGE VELOCITY HEAD. i». KjO
Mutism VELOCITY HEAD, «. KjO
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DRY MOLECULAR WEIGHT DETERMINATION BY
SAMPLING TIME (21-h( CLOCK)
SAMPLING LOCATION
SAMPLE TYPE (DAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
AMBIENT TEMPERATURE
"^^^^ RUN
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PROJECT NUMBER 37=>/
-141-
TEST NUMBER ^ FIELD DATA SHEET
J! SCOn ENVUONMENTAl TECHNOLOGY. IMC
PROBE LENGTH 4 TYPE H
NOZZLE I.D. .?V; "
PLANT flty^^ &r.*^JC.Jf,,
DATE * //. /«r-7^ ^
SAMPLING LOCATION Ly-.^..-., <£.... ili-v - •J,.,,.'./',. SAMPLE BOX NUMBER .\l,s.'-f. £./
SAMPLE TYPE '),'i,f/. 7 < - ^ rt .'.f.-f METER BOX NUMBER v 1} 1?,./.
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AMBIENT TEMPERATURE £Z REFERENCE iP .SO
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l.lo A //
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CO, 0, _
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-142- NOMOGRAPH DATA BY
JQI5TURE
KPINGERS
FINAL VOLUYE
IMTIAL VOLUME
BET VOLUV.E
ANALYTICAL DATA BY
Vll
BF
ol
i:!
SILICA GEL
FINAL WEIGHT
INITiAL KEIGHT
NET WEIGHT
TOTAL MOISTURE
2.76.^
-£J
L£>£
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mg
mg
mg
mg
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mg
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mg
mq
mq
'i^
mg
ACETONE BACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NET mg
WATER EVAPORATION
FINAL ' mg
TARE mg
NET mg
TOTAL BACK mg
I CERTIFY THAT THE SAMPLES OESCP.I3ED
BY THIS DATA SHEET WERE COUECIEO IN
ACCORDANCE 'WITH HETHCOS OUTLINED 8Y
WIPE IN THE POSSESSION OF, C8 SEALEB
FOR SHiPSE.NT EY CUMW CARRIER SY.
KYStLF UNTIL DELIVERY TO A LABORATORY
SIGNED DATE
UITIESS KTE
\ i ctRTiFTTwmtcnTm?! SASI-ITS
} DESCPI3ED Ef THIS DATA SriEE! FROf. IHE
J ABOVE NAMED [V)!VIU.'-L AnO ANALYZED
THEM IN ACCCSD^ICE WITH THE A20VE
NAME 3 PROCtO'JPE.
MLI6HATEO PRESSURE DIPFtSEHTHL ACROSS
ORIFICE, to. «;0
AVERAGE KTES TESFERATURE (Ase:£f(T *n*f).'F
PEF.CEHT K3ISTURE l» CAS STREAK 8» VOlUtlE
BARBIETRIC PBESB3E AT KETER. In. h(
STATIC PRESSURE IN STACK, la. H|
P,i^.«?1 1 STACK GAUGE PRESSURE in in. «;0)
RATIO Of STATIC PRESSURE TO «£TER PRESSURE
AVERSE STAGS TLV.PCRAlUfit.'F
AVERAGE V4CCITY HEAD K KJ!
vMuioa vriocrn HEAD. in. H2o
C FACTOR
CALCULATED NOZZLE OIAYETER. in.
ACTUAL IOZZLE DIMETER, in.
RF.rERE.VC-: ij. in. H,0
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DRY MOLECULAR WEIGHT DETERMINATION BY
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ANALYTICAL METHOD
AMBIENT TEMPERATURE
T-
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-------
PROJECT NUMBER ;-".->/ TEST NUMBER >. FIELD DATA SHEET
PLANT £,£.„,, P.«,y,-.-/, PROBE LENGTH 4 TYPE '.';...-* ,,2,^
DATE v"?!^- I5J.\*T>. NOZZLE I. D.
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STACK
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EMPERATURE]
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, COC.MENTS
-------
-144- NOMOGRAPH DATA BY
IQISTURE
KPINGERS
FINAL VCLIKIE
INITIAL VOLUME
NET VOLUME
. Bl
.ml
.si
SILICA CEL
FINAL WEIGHT
INITIAL WEIGHT ^ ' •-'. '•' | '•> i. 3
NET WEIGHT j 1 • ** !
TOTAL MOISTURE iM
ANALYTICAL DATA
BY
ACETONE FRONT WASH
FINAL «/S".( '^4-9 mg
TARE
NET .
FILTER
f(J< FINAL
fl> TARE..
e\
JT frjn'*>l, mg
1 1 \.(i ' ma
NUMBER 1
.4130 ^
1 *
3 .<•?<• / mg
i i « ^- mg
FILTER NUMBER 2
FINAL
TARE
NET
mg
mg
ma
FILTER NUMBER 3
FINAL mg
TARE
NET
CYCLONE
FINAL
TARE
NET
TOTAL
" \5v •**
prr^-r
.::.:....|r
w
SJSp
r-rk"- ;
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C-8«NIPPLE
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rt ,,
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tM
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/ mo
FRONT 155T.?X mg
•»<*'
^ENTAl TBCMNOtOOV, INC-
{ *
|,:::r~.t
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r-:-f~
:::.l
—:••—:
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:~J..::^::~t:ii:
:";r"~ti~rr=-:
ACETONE BAC!< WASH
FINAL
TARE
NET
ETHE
mg
mg
mo
R-CHLOROFOR.H EXTRACT
FINAL
TARE
NET
mg
mg
mg
WATER EVAPORATION
FINAL .
TARE
NET
mg
mg
ma
TOTAL BACK
mg
I CEBT ft THAT THE SWLE
BY THIS DATA SHEET 'J:Rt C
ACCORDANCE W,'TK KPS-WS 01
WERE S THE POSSESSION If
F0°. SHIPMENT Br CCrt-OS CA
KY5ELF UAiTi. DELIVERS TO
FOR ANADSIS.
SIGNED
S OE
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0
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NED BY
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SEALED
1 BY.
SCflATORY
«TE
^IIT^ESS MTE
I C£»T!'( "Hi* 1 SrtJi^C THE SASfLfS
DESCRI2VC EC THIS DATA SKEST FRO« *HE
ABOVE .WED IKOtvltML AND MALViEO
THEM IN A:CO=."-NCt W TH THE ABOVE
KAMED «O:EDUS:.
.. SIGNED DATE
WITNESS
iSHr;.
M
.07) i STACK GAUCE f 3ESSUHE in in. Hjd)
RATIO CF STATIC PRESSUSE TO KETER PRESSURE
AVERAGE STACK TC:-?ERATURE. 'F
AVERAGE VELOCITY HEAD. ii. HjO
«AX SUM VELOC TY BEAD. in. HjO
CFAC
TOS
CALCULATED KOZ21C OUSTER, in.
ACTUAL MULE DIMETER, ».
REFERENCE ij. in. KjO
DRY MOLECULAR WEI
SAMPLING TIME (24-hr CLOCK
SAMPLING LOCATION
',
V.
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GHT DETERMINATION BY
}
SAKPLE TYPE (BAG, INTEGRATED, CONTINUOU
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AMBIENT TEWPERA
1
^\_^ RUN
GA! ^^^
-v
C02
KC.40!.% KMUS ACTUAL
CO; READING)
READlCC SiSltt ACTUAL
02 AEADthC)
-------
-145-
PROJECT NUMBER ^-' TEST NUMBER
PLANT 0~\ tj^Axo l?>ir-
METER BOX NUMBER
^
-7 S'c- . jtj 9
f*-
RAVER;E
PUT
.1UY.BIR
CLOCKI
CiS JEIER F.UD.'.IG
(V.l. It3
VELOCITY
HEAD
l»,l. 0. KjO
ORIFICE rEESSJRE
DlfFEREKTKL
DESlRtO ACTUAL
3?
STACK
EiVERAT'JSE
ORYCM^ETER
TE.IPERATURE
I«LET_4_CUTLEL
UL
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ACUIM.
in. H|
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60
-------
J.IOISTURE
BPINGEP.S
' FINAL VOLUME
INITIAL VOLUME
NET VOLUME
FILTER NUMBER i
FINAL
TARV
-NET
FILTER NUMBER 2
FINAL
TARE
NET
FILTER NUMBER 3
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET
-146- NOMOGRAPH DATA BY
SILICA ca
FINAL WEIGHT *-''*>.& ,
INITIAL WEIGHT Z-!»fo..r ,
NET WEIGHT
TOTAL MOISTURE
ANALYTICAL DATA BY
ACETONE FRONT WASH
FINAL 33. bSOS" mg
TADC f\. "3 f—f y" J MI
IMKt ^ *; j (^ cj. ^ / my
NET 1 0 -1 mg
jng
_mg
_mg
_mg
_mg
_mg
_mg
_mg
mg
jng
jng
TOTAL FRONT
nig
ACETONE BACK HASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NET mg
WATER EVAPORATION
FINAL _.
TARE mg
NET mg
TOTAL BACK mg
i CERTIFY TH;; THE SMPLES OESCSISED
BY THIS QAU Sr^tT '.'F.^E COLLfCItD IH
ACCORDANCE WITH nances OUTUKO BY
WFPE !N THE POSSFSS.'C't OF. 03 SEALED
RVStLF WTIl OCLIVcP.Y TO A LA90MIOHY
FOR AKAIISIS.
SIO.'IEO
_OATE_
CATS
WITKE5S _
i cERTirnTiAT r&itrnttr
DESCRIBES 2Y THIS :ATA SHEET FRa^ THE
A30VE SA.«iO DiniVIOL'AL Ah'O A.1ALYI-D
TKl',1 IS ACCOF.DA.SCE WITH THE ASOVE
hAHED PROCEDURE.
SCOTT ENVIRONMENTAl TECHNOLOGY. INC.
SIGNED
DATE
CALI3R>TED PRESXK CIFfERE.HTIAL ACROSS
ORIFICE, in. -jO
«VE«Ar,ErEIEfiTEyPERATURE(MBlEKT»n'F).'f
PERCL-ST IWSTUF.E HI C'S STREAM tY VOLIBE
BAROMETRIC PRESSURE AT "ETER. in. Ml
STATIC PRESSUR: IN STACK. i«. H.(
P,i^.«J ; STAC1 CSL'CE PRESSURE in in. KjO)
RATIO OF STATIC PRESSURE TO *ETER PRESSURE
AVESACE STACK TK'PERATU3E. 'f
AVERAGE VELOCITY HEAD. in. HjO
KAXlYUt VELOCI1Y HEAD. in. HjO
C FACTOR
CAUUUUD KOZZLE DISVETER. in.
ACTUAL KOZZLE DIAMETER, in.
REFERENCE It. in. H;0
'».
T-n
«w
'.
',
V.
TW
",„.
«»«!.
.f
-------
PROJECT NUMBER 2-7"
PLANT f^L^j^ *3 o-
DATE " '////rV 7 9
SAMPLING LOCATION £.«-
SAMPLE TYPE <~
RUN NUMBER J"""
OPERATORS btt_) J ^
AMBIENT TEMPERATURE
/ TEST NUMBER ^' FIELD DATA SHEET /rsisc
V/i
-*.b*J PR03E LENGTH 4 TYPE 7 X " ^
NOZZLE I.D. , >7_i
,L^L Vw^.^t< liu.'tfcC SAMPLE BOX NUMBER ^-cc-C^ -5,
METER BOX NUMBER /? F} <- '2—
PROBE HEATER SETTING 2 2- V^ -
— FILTER HEATER SETTING -2.2- 5"
^ j" REFERENCE iP /Xf
SCOn JNVIIONMENTM HCKNCHOGY. IMC
FYRITE ANALYSIS
CO, 0, _
BAROMETER
READ AND RECORD ALL DATA EVERY 3— MINUTES PITOT NUMBER .
RAVERSE
POiM
KIOTO*
CLOCK TI».E
SHrpLIKC i
IIVi.«m CLOCK)
CAsrETERREAoms
(V.'.H1
INITIAL: .t
VEICCITT
HEAD
l;,l. b. HO
DESIRED
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TE>.'ER*TUR£
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"frc6i
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-------
-148- NOMOGRAPH DATA BY
JWISTURE
BIPINGERS
FINAL VOLUME ?- ' ~>
INITIAL VOLUME _k
KET VOLUME
ANALYTICAL DATA BY
ACETONE FRONT WASH
FINAL r
TARE
NET . 3_
FILTER NUMBER 1
FINAL .^(V?.3
TARE.,
lEf1
FILTER NUMBER 2
FINAL
TARE
NET
FILTER NUMBER
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET
SIUCA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
TOTAL KOISTUHE
_"ig
jug
_mg
jng
jng
__ng
_mg
_mg
jng
mg
mg
ACETONE BACK HASH
FINAL ' mg
TARE _. mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NET mg
WATER EVAPORATION
FINAL ^ mg
TARt mg
NET mg
TOTAL BACK mg
1 CERTIFY TH« THE SWLES DfSCKiBED
BY THIS DATA SHEH i£?i COLUCU3 I.I
ACCOSCA.SCE WITH «Erri035 OUTLINED BY
rrartME^cEHTiFf nurwuBPiET
VEK III THE POSSESSION OF, 08 SEALED
FOR SHIPMENT BY CC.'T'CN CARr'iER E'.
K'l'SELF Li'lTIL CELNESY TO A LABORArORY
FOR AXALYSIS.
SI'jHED DATE
TOTAL FRONT
SCOn ENVIRONMENTAL TECHNOLOGY. INC.
WITNESS
KTE
fc!!/;5 THE inSPtrs
DESC'IDEO BY THIS tVH SHEET F?0« THE
ABOVE tAMEO ES^IVID'.'AL S->iO ANALYZED
THE^ IS ACCORDANCE WITH TriE ABOVE
•A.MEO reoCED'-RE.
SIGNED
DATE
UUBSArEO FRESS-JRE Olf FEFEKT'AL, ACROSS
ORIFICE, ». B;0
*V£R«E «EI£R TCKPEMTURE (MBIE«T»»*n.'F
PERCEST V_)i!TijR= « CAS STREW sr VOLIKE
SARO'JETRlC PBEiiiiaE AT BETER. in. HI
ST«IIC PRESSURE IS '.TACK. !«. HI
P,±|.3!J I STACK GAUGE PRE!Sl"!E i.-. in. H;0)
RATIO Of STATIC PRESSURE TO BETER PRESSURE
AVERSE STACK TEi'PERATUSE. *F
AVERAGE VELOCITY K- AO. in. Hf
KAXIXUX VELOCITY HEAD, ii. K;0
C FACTCR
CAICULATEO N0221.E DIAMETER, in.
ACTUAL KIZLEDUV.EICR. i».
REFERENCE in. in. l-jO
««f
T'««.
B»
'.
P,
V.
T..,,
4»i,(.
'frji.
DRY MOLECULAR WEIGHT DETERMINATION BY
SAMPLING Tfi.IE (24-ht CLOCK)
SA.MPLING LOCATION
SAMPLE TYPE (BAG. INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
Wi'.BIENT TEMPERATURE
\^^^ RUN
GAS ^\^
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PROJECT NUMBER .3-?°
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SAMPLING LOCATION
SAMPLE TYPE *
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TEST NUMBER FIELD DATA SHEET
PROBE LENGTH & TYPE 73,
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-150- NOMOGRAPH DATA BY
MOISTURE
BPINCERS
FINAL VOLUKE .?-<> a\
INITIAL VOLUME Ji±<2_ nl
HET VOLUME /7 , ol
ANALYTICAL DATA BY
SILICA ca
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
TOTAL MOISTURE
Z1S.S
3o
ACETONE FRONT WASH
FINALS 0. kA-f<^
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FILTER NUMBER 1
FINAL V37b1
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FILTER NUMBER. 3
FINAL
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CYCLONE
FINAL
TARE
NET ^^
TOTAL FRONT ' ^ i '^
mg
/ mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
.rag
> / >
SCOn ENVIRONMENTAL TECHNOLOGY. INC.
ACETONE BACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE . mg
NET mg
WATER EVAPORATION
FINAL mg
TARE mg
NET mg
TOTAL BACK mg
1 CERTIFY THAT THE SAHPLES DESCRIBED
BY THIS DA7A SHEET WERE COLLECTED IN
ACCOROA.'.CE tilTH HEIHOOS OUTLINED BY
WERE IN THE POSSESSION Of. OR SEALED
FOR SHIFMEM BY COMMON CARRIER BY.
KYSELF U.MIL DELIVERY TO A LABORATORY
FOR ANALYSIS.
S1SKEO DATE '
WITNESS OA.TE
1 CEBTIFY TPA! I RHnTOTTfE SAKFTTS
DESCP.IS10 BY THIS DATA SHf.ET FP.OK THE
«BOVE SIKO INDIVIDUAL A»0 AIULVZEO
THEM IN ACC053A.1CE WITH IHE ABOVE
«A»£0 FSOCEOi,SE.
SK^EO BATE
WITNESS 0«IE
CALIBRATED PRESSURE OtFFERESTIAL ACROSS
ORIFICE. !n.«jO
AVERAGE KETES TEHTERATURE (,V18:E*T •E"F).'F
PERCEilT KOISTURE 1* OS STREAM 8r VOLUKE
6AROVETRIC PRESSURE AT CETER. l>. HI
STATIC PRESSURE » STACK, in. H|
tf^.m . STACK GAJGE FRESVJBE in ». H;0)
RATIO CF STATIC PRESSURE TO KSTER PRESSURE
AVERAGE STACK TEMPERATURE. °F
AVERAGE VELOCITY HEAD, m. HjO
BAXW.IW VELOCITT HEAD, in. H;0
C FACTOR
CALCULATED NOZZLE DIWETER. in
ACTUAL KOZZLIOI.V.:EIER. in.
REFERENCED, in. H;0
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SAMPLING TIME (2Ut CLOCK1
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BY
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ANALYTICAL METHOD
AMBIENT TEMPERATURE
"^\^^ RUN
GAS ^^^
C02
02;.-
-------
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PROJECT NUMBER ti^i TEST NUMBER "7
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-152«OMOGRAPHDATA BY
MOISTURE
tiPINGERS
FINAL VOLUME
BIITIAL VOLUME
HETVOLUME
ANALYTICAL DATA BY
A_CETONE FRONT WASH
FINAL /0«2.-)-7i.O
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TARE
NET
ACETONE BACK WASH
FINAL rag
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NET mg
MATER EVAPORATION
FINAL mg
TARE mg
NET mg
TOTAL BACK mg
jng
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1 CERTIFY THAI THE SWLES OESCRI3EO
BY THIS OAIA SHEET VESE COLLECTED IN
• ACCOSCANCE WITH HETHCOS CUTLIftErj BY
VE.1E IN THE POSSESSION Of. 0? SEALED
FOR SH.'PHE.ST BY CO^CN CARRIED 5i',
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NOHOGRAPH DATA BY
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BIP1NGERS
FINAL VOLUME _i2fLiLinl
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NET VOLUKE _ -'*• el
ANALYTICAL DATA BY
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JILICAGEL
FINAL WEIGHT JgfQQ. t
INITIAL WEIGHT _iki±. t
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TOTAL KOiSTURE j?
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(ip.l.o.HjO
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OSIFICE TRESSUBE
OIFFESEMIK1.
ESSRtO
ACTUAL
•-.
•- -.
STACK
Ei'.PERATURE
fT.I.'F
N
DRYCtSyETER
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MOISTURE
HPIHGERS
FINAL VOLU"£
INITIAL VOLUME
KET VOLUME
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET HEIGHT
TOTAL MOISTURE
ANALYTICAL DATA BY
ACETONE FRONT WASH
FINAL >:\ I O4?.Q
TARE 89.'J/£Tfe /
'"El . UlL.T7^
mg
mg
FILTER NUMBER }
FINAL .
*? 7 • D
NET
FILTER NUMBER 2
FINAL
TARE
NET
_mg
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_mg
_mg
_mg
_mg
FILTER NUMBER 3
FINAL
TARE
NET
_mg
__mg
ng
ACETONE BACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL .mg
TARE mg
NET
WATER EVAPORATION
FINAL j
TARE
NET
TOTAL BACK
mg
_mg
_mg
mg
__mg
1 CERTIFY TrUT THE SAXPLES DESCP'.SEO
BY THIS DATA SfEEi WERE COLLECTED IN
ACCORDANCE VIIH KTiiOOS OC'TLINEO 81
Vlfli IN THE POSSESSION CF, OR SEALED
FOK SHIPMEN- 31 C0l«» CARRIER 3Y.
MYSELF UNTIL ElLIVEiK TO A LABCU70RY
FOR ANALYSIS.
SIGNED
_OATE_
CATt
WITNESS
I CEI
DE5c?isfD sr THIS DATA SHEET .C:?OM THE
A30VE NAMED INDIVISL'AL i'O A'iAUitD
THEM IN ACCOJDWCE WITH THE ABOVE
NAnO PROCEDURE.
SIGNED
_OA7E_
DATE
NOMOGRAPH DATA BY
CALIBRATED PRESSURE ClFFEREHTIAl ACROSS
ORIFICE. In. HjO
AVERAGE rtTERTE*P£RATUE£(AY,EtEIn
'.
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'•..,.
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DRY MOLECULAR WEIGHT DETERMINATION
SAMPLING TIKE (24-hi CLOCK)
SAMPLING LOCATION
BY
SAMPLE TYPE (RAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
AMBIENT TEMPERATURE
^\^^ RUN
GAS ^\^
C02
02(HET IS ACTUAL Of
r.£AOiac rt.tus ACTUAL
COj fiEAOISC)
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SAMPLING LOCATION frutjt ic^fa-T £?/_£.'•"•:? SAMPLE SOX NUMBER /! -L.^t
SAMPLE TYPE
•
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FYRITE ANALYSIS
CO, 0,
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?UN NUMBER 7 PROBE HEATER SETTING - '
DPERATORS /Re - T6 FILTER HEATER SETTING A'//!
WB I ENT TEMPERATURE C-7°^" REFERENCE iP
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TRAVERSE
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SAXPLING
ICS Tl.Vt
CLOCK!
CAS JETEP READING
IV.I.B1
.
VELCCTTY
li»,l, in. H^O
OfllFICE PRESSURE
DIFFERENTIAL
DESIRED
ACTUAL
STACK
TEMPERATURE
rt,i.'F
TEfJERATUFE
IfiLET
in. H(
•
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FILTER NUMBER }
FINAL • "3
3 6 Ay
NET _. i
FILTER NUMBER I
FINAL
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FILTER NUMBER 3
FINAL
TARE
NET
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MOISTURE
RIPINGERS '
FINAL VOLUME
INITIAL VOLUME .2.r-'
NET VOLUME -ZL
ANALYTICAL DATA BY
ACETONE FRONT WASH
FINALES'.!
TARE
NET
SILICA GEL
FINAL WEIGHT gfi/,3 f
INITIAL WEIGHT £J^.i2_ I
NET KEIGHT *••>•'
TOTAL MOISTURE
mg
mg
_mg
_mg
_mg
_mg
_mg
_mg
_mg
jng
jng
-ma
•i mg
4
ACETONE BACK WASH
FINAL rag
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL
TARE
NET
WATER EVAPORATION
FINAL
TARE
NET
TOTAL BACK
mg
mg
_mg
mg
mg
mg
1 CERTIFY THAT THE iAy^LtS CESCPtOtfl
8» THIS OATS SHEET WE'E CDLLECTCO IS
ACCORDANCE W!TH KCTItOOS (MIL IKED BY
I FURTHER CESTI-Y :^7
WERE IS THE POSSESSION Gr. OR SfAlED
F0» ShlPK1.? B> VOV» CARRIES SI,
WSELF UNTIL DELIVERY 10 A LAEO'AIOBY
FOR AMLYSIS.
SIGHED
DATE
AIt
TOTAL FRONT' V/0.\
SCOn SNVUONMENTAL T£CHNOIOGY, INC.
WITNESS
1 CERTi.-Y
DESCRIBED BY THIS [1ATA SHEET FROM THE
ABOVE SWtO nniVirJL'AL AliO AWl TZEO
THES IN ACCM3A.1CE Wit THE ABOVE
KAMEO FROCEDUPI.
SIGNED
DATE
NOMOGRAPH DATA BY
CALIBRATED PSESSU2E DIFFERENTIAL ACROSS
CfliFICE, ta.H;0
«V£H1£ f ETER It.«f EF.ATURE (AWIENT »n'FVF
PERCENT KOISTURE 11 GAS STREW BY VOLIKE
BAROKETRIC PRESSURE AT SETER. IB Hj
STATIC PSESSURE 111 STACK. i(L HI
P.i^.WJ i STACK 5AUCE PRESSURE in in. H2c)
RATIO OF STATIC PRESSURE TO KETER PRESSURE
AVERAGE STACK TEMPERATURE. 'F
AVERAGE VELOCITY HEAD. i«. HjO
KMISIH VELOCITY BEAD, in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER. i«.
ACTUfL KOZZLE DIMETER, is.
REFERENCE if. in. H20
4Kf
T'»«.
««
'.
P,
V.
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DRY MOLECULAR WEIGHT DETERMINATION BY
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION
SAfuPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL KETHOO
A.VDIEHT TEMPERATURE
RUN
COfhfT IS*C)«ALCO
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AVERACE
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INSIDE DIMENSIONS OF SAMPLE PLANE
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STACK GAUGE PRESSURE 1n. HyO-a^^"
NEAREST UPSTREAM DISTURBANCE 2&
NEAREST DOWNSTREAM DISTURBANCE Zu"
PROCESS & CONTROL EQUIPMENT
DESCRIPTION
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TEST NUMBER Q FIELD DATA SHEET
DATE <" y. - /-/.V7V--
PROBE LENGTH i TYPE
NOZZLE I.D.
SCOn CNVIIONMENTAl ItCMNOtOC*. IMC.
FYRITE ANALYSIS
CO,
SAMPLING LOCATION
SAMPLE TYPE ',-f..-//../ ^T
RUN NUMBER f /' , . ...
OPERATORS /\>r • _''
A^L
•.A.MBIENT TEMPERATURE
BAROMETER 2 ( .
SAMPLE BOX NUMBER -'•
METER BOX NUMBER "'_?
PROBE HEATER SETTING _
FILTER HEATER SETTING
REFERENCE iP •>.«•
READ AND RECORD ALL DATA EVERY
.'->.: ~f~ -f f.
MINUTES PITOT NUMBER.
' -••./..-i--.;
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CAS JETER REAOinC
(V.I.It1
VELOCITY
HEAD
tlj,l. n. KjO
ORIFICE PRESSURE
OIFFE5ESTIA!.
DESIRED
ACTUAL
STUCK
TD7ERATUSE
ft.l.'F
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-------
-160-
NOMOGRAPH DATA BY
MOISTURE
KPINGERS
FINAL VOLUME ' " ~) r.l
INITIAL VOLUME - '' ml
HET VOLUME _rii_ ml
ANALYTICAL DATA BY
SILICA GEL
FINAL WEIGHT ^"
INITIAL WEIGHT _1_
NET KEIG.'iT L
TOTAL KOiSTUftE
ACETONE FRONT WASH
FINAL 8 is,/ O~)(f,
TARE 8b.G> f?7.1.
NET . 2. S . f
FILTER NUMBER 1
FINAL .•a.fcaxj-
TARE.-P'. .? .5" rt C"V
•NET" I.")'
FILTER NUMBER 2
FINAL
TARE
NET
FILTER NUMBER 3
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET .- ;
TOTAL FRONT ; I^V
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mq
7 ~-
'^~mg x
mg--
ACETONE BACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NET mg
WATER EVAPORATION
FINAL mg
TARE mg
NET mg
TOTAL BACK. mq
I CERTIFY THAT 1XE SWWES DESCRIBED
BY THIS PATA SHEET WERE COLLECTED IN
ACC^.CANCE WITH f.ETH&DS OVTLI.NED BY
UEBE 1\ TVE F-OSSESSIOH OF. OR SEiLED
FOS SHIPVEM SY CO^CN C-5RP.1ER i!Y.
Kl'SEIF ONIIL DELIVERY T'J A LASO»JTCR»
FOR ANALYSIS.
S1G«EO OAIE
WITNESS WTE
I CERnfV Js-r 1 ?.!cE!v'i' THE SABLES
OESCSI3EO 3« THIS WTfl Sv.EET FROM THE
ABOVE NAMED INDIVIWAL WD A.NAIYZEO
CSJLIBVTED P3ESS-J3E DIFFERENTIAL ACSOSS
CRIf ICE. it. HjO
AVERAuE JETER T£*?ERJTL'SE(AWSIEH'r»ra'F).IF
PERCENT (COTSE is c»s STREAS sr VOLUME
BARJBETfJC PRESSJSf *T KETES. it. HI
STATIC PBES'Uf!- 11 STUCK, in. H|
P.^.Oli I SUCK CAUSE PRESSURE « In. H;o)
RATIO Of STATIC PRESSURE TO KETER PRESSURE
HVJSAGE STUCK TEZFERkTUP.E. 'f
AVERAGE VELOCITY HEAD. in. »f
XAXIbM VELOCITY HEAD, in. K;0
CFACI08
CALCULATED NOZZLE L'lAV.ETcS. is.
ACTUAL KZZLl CI«:ETER. h.
REFERENCE 3p, in. HjO
» >
'.
f,
V.
V
*'««.
»»«•.
DRY MOLECULAR WEIGHT DETERMINATION
SAMPLING TIME (24-hi CLOCK)
SAMPLING LOCATION
BY
SMiPLETYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
AMBIENT TEMPERATURE
ACC::;-CANCE WITH f.ETH&DS OVTLJ.NED BY
I F'j;i!iE= CEPTtFY THAT Tl'E SAX'ltS
UEBE 1\ Tf'E F-OSSESSICM OF. OR SEiLED
FOS SHiPVEM £Y CO^CN C-5RP.1ER i!Y.
Kl'SElF ONIIL DELIVERY T'J A LASO»JIC«Y
FOR AjSALYSIS.
S1G«EO OAIE
WITNESS WTE
OESCS!3LO 3« THIS WTfl Sv.EET FROM THE
ABOVE NAMED INDIVIWAL WD A.NAIY2EO
THE1 IS ACCCUA»CE UIIH IKE ABOVE
hA.1EO PROCEDURE.
•SIGNED DATE
WIT«« OA1I
^^^_^ RUN
^~
GAS ^^^
C02
0;(NETIi ACTUAL 0;
CO; REAOtfCt
CO.NETISACT'JAtCQ
REiOiKC SiMU ACTUHL
Ct READiNQ
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1
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liET
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VOLUME
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PLANT CM *H>M 6 -M c(>J PROBE LENGTH &
DATE (1 «///(. A? Cf ^ NOZZLE I.D.
TYPE 7--V " «i/ FYRITE ANALYSIS
/*-" ^
« ?7 V
CO, 0,
SAMPLING LOCATION I^A i*+J&f- c?.2-^~
AMBIENT TEMPERATURE A 7 REFERENCE iP
BAROMETER
TRAVERSE
&f '
2.
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2_
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RECORD ALL DATA EVERY > MINUTES
ORIFICE PRESSURE
DIFFEREBIIAL
UK), in. KJ})
OESiREO
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Air
Af-T
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-------
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^
MOISTURE
WPINGERS
FINAL VOLUl'E
INITIAL VOLUME -
BET VOLUME ~ '
.ml
.ml
.ml
SILICA GEL
FINAL KEIGKT
INITIAL HEIGHT '.2.to3.3 J
NET Ki'EIGKT ! 7'"- <
TOTAL MOISTURE. */_
ANALYTICAL DATA BY
ACETONE FRONT WASH
FINAL feU. 7. 01 |
TARE Sk .I'gA-'a,
NET ' I'L.S '
FILTER NUMBER 1
FINAL ,1,70^-
TARE __-t> , ^ b f?O
NET M'
FRTER NUMBER ?
FINAL
TARE
NET
FILTER NUMBER 3
FINAL
TARE
NET
CYCLONE
FINAL
TARE
NET ./'^-~T
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
-mg-.
ACETONE BACK WASH
FINAL mg
TARE mg
NET mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NET mg
RATER EVAPORATION
FINAL mg
TARE mg
NET mg
TOTAL BACK mg
1 CERTIFY THAT THE SWISS DESCRIBED
BY THIS DATA SHEET iESE COllrCTEO IK
ACCOJIWCE WITIi METHODS Sl/IU.'.EO 6*
UERE IN THE POS^ESSICS OF. 0? SEALED
FOS ShIPttH S> COWOK CARRIER BY,
MYSELF UNTIL OELIVEP.Y TO A LA30°ATORY
FOR AMIISIS.
SIGNED DATE
VITNESS MTE
i cEFrimBsTTennvsirriit SA?>TTS
TOTAL FRONT,''
TV?
;£D 5V THIS DATA SH^ET FnOM THE
ABOVE NAKED ItOIVJOUAL -VJD A.NALYZED
THEM IN ACCOr\D;jiCE WITH THE ASOVE
NAMEC PROCEDURE.
SCOTT ENVIRONMENTAL TECHNOLOGY, INC.
SIGNED
DATE
NOMOGRAPH DATA BY
UL.'ESATEO PRESSURE DIFFERENTIAL ACROSS
CRIFICc, In.KjO
AVERAGE SETER TEXPERATUSi (W3IEHT t a'Fl.'F
PERCENT MISTIME IK CAS STSEAS BY VOLUSIE
BARCWETRX FSESS'JAE AT KCTER. It. «t
STATIC PRESSURE IN HACK. a. H|
P,i^.OH 1 STACK. CRUCE PRESSWE » in. H2Ci)
RATIO OF STATIC PRESSURE TO KETER PRESSURE
AVERAGE STACK TEI.TERATL-fiE. °F
AVERAGE VELOCITY HEAD, ir.. Hf
XAXWUa VELOCITY HEAD, in. Hjil
C FACTOR
CALCULATED BOm-E DUSTER, in.
ACTUAL K522LE CIMETES. ia.
REFERENCE if. in. K20
»««
'•••-
««
'.
',
V.
'•„,
«'»l.
»»„.
(
1
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o"liE
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— "1
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(J* "*
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-------
-163-
• , • PROJECT NUMBER 2.7 <»/ TEST NUMBER
1
_ * i
4V .i f
.1-1 > [
LANT ///
FIELD DATA SHEET
'rtf~j & C "2-
RUN NUMBER (f PROBE HEATER SETTING 7. •*.•"-
OPERATORS 0 ({/ -S> ^ FILTER HEATER SETTING 7- 2- T"
.• AMBIENT TEMPERATURE
; BAROMETER
-VJ--
'.V ' V-
w .-
'** :T * ' *"'
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5
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3
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TRAVERSE
MUYBER
J/ 7 REFERENCE iP
/. (
2 ^ , 1-4 READ AND RECORD ALL DATA EVERY 7 MINUTES
CLO
SMPLikC
Tli'c.Bl.1
7
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?-?
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7(5. "S7/
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^^ ^ _
- — ^
CAS f.ETER READING
(V.I. ^
VELCCITT
HEAD
ORIFICE PRESSURE
OIFFEBEMIAI
UH). a. NjOl
DESIRED
«•*?,
,3
lib
1.0
/,$
/,Yf
/•^
/ y
AC1UAL
/7-
O
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•2.0
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^
STACK
!E*?ER»TURE
''
5"2_
rK
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$T)
(f '3
"7 (
11
10
UVS'iv
*
s*-**?:^ ^.
05IFICE PF.ESSJBE
DIFHSr.lTIIL
DESIRED
ACTUAL
STACK
TE.WERATURE
ORrCUKETER
TLVERATURE
INLET
•¥&'
r^
61
7 ~
(f 7
7-fc~
7r
10
OUTLET
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6 7
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PUYP
VACUia.
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7-
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"F
60
Co
to
60
00
b 5
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Tsr^w^-^— «^J-
DSfCASYETCR
TEYPERATUF.E
IKLET
-OUIIEL
Pur^P
VACUUM.
EKPERAI
"F
PITOT NUMBER
?il
COMMENTS
LTW< ,o-L LrH lf"/{(
<4.
(
1.
*.
^^^ , V
• ' " " - ""-•- ~
URE]
COMMENTS
-------
-164-
NOMOGRAPH DATA BY
.MOISTURj
KPINGERS
FINAL VOLUME ~2J*° nl
INITIAL VOLUME ^-o-n nl
KET VOLUME 1? ml
SILICA ca
FINAL WEIGHT
INITIAL WEIGHT
NET TiEIGHT
TOTAL KOISTURE
"Tjiv.v t
~/
ANALYTICAL DATA
ACETONE FROUT WASH
FINAL c
TARE 'Bl.^Tl'A'^
NET . "i T>.
FILTER NUMBER 1
FINAL . , mg
i m3
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
mg
"^TrfgN
mg '
SCOn ENVIRONMENTAL TECHNOLOGY, INC.
FINAL
TARE
NET
ETHER-CHLOROFORM
FINAL
TARE
NET
mg
mg
mg
EXTRACT
mg
mg
mg
WATER EVAPORATION
FINAL mg
TARE
NET
TOTAL BACK
I CERTIFY TWIT THE SAy?
BY THIS DATA S'ictT WERE
ACCOHMNCE WITH KErriCOS
WERE Ifi THE POSSESSION
FO? SKiMENT Bl CO'W.f
HISELF UtiTIL CELIV£« T
FOR ANALYSIS.
WITNESS
I CERTin-TBrTTfcTlv
KbiisUHS IV.iViP.'AL
TRL». ii jccestw.c- WITH
KAHEO PROCEOURE.
SIGNED
WITNESS
mg
mg
mg
LES DESCRIBED
COLLECTED IN
OUTLINED BY
Of. 05 SEALED
CS8RIES 5Y.
0 A LABORATORY
DATE
DATE
mft SASSTTS
SHEET FRJ- THE
~THE"AEOVE
DATE
DATE
CALIBRATES PRESSURE DIFFERENTIAL ACSOS!
ORIFICE, ta. H;G
AYF.RAGE r£"E.t TEWERATUSE (.,
V.
T,
•i»l.
'•.„
»»«..
DRY MOLECULAR WEIGHT DETERMINATION BY
SAMPLING TI.VE (2J-hr CLOCK)
SAMPLING LOCATION
SM-PLE TYPF. (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
A.V.BIENI TEMPERATURE
^^^^ RUN
GAS ^\^
C02
02;NFTIS ACT'Ji-LCj
Rf*Cl.15 rif'jS ACTm
COj fiEASl.'tC)
CO'htT IS HCrjAL CO
R£.Au:;;GXiMJWgitJAL
Oj ?.t;.&wct
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AC1UAL
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SET
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mmm
liiliiiSi
:::::.-.-:.-):-.—: r.--
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£ )r
a r*
LU r>
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STACK GAUGE PRESSURE in. H?0— ,3./
NEAREST UPSTREAM DISTURBANCE
NEAREST DOWNSTREAM DISTURBANCE
PROCESS & CONTROL EQUIPMENT
DESCRIPTION
; 3
;
s
3
«
*r
ENVIRONMENTAL TtCHNOtOGY, INC.
O
a:
-------
•r- -. • -165-
PROJECT NUMBER 2-'° ( TEST NUMBER
i
-,
t
(
/
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t
i
i
i
i-
^
i
'LANT Ov-^
FIELD DATA SHEET
.A fcc~, /^ _ PROBE LENGTH & TYPE P--t- " °rf
3ATE ]t/,-i{-iAMPL1NG LOCATIONT^Ji tYic^t" ^-cJ^fefe SAMPLE BOX NUMBER S-<^T ^ J>
JAMPLE
TYPE
T METER BOX NUMBER £Ll\-
U1N NUMBER ^ PROBE HEATER SETTING •? 2^ .
OPERATORS ^f 3 r FILTER HEATER
WBIENT TEMPERATURE 7O REFERENCE iP
JAROMETER 1 6.
TRAVERSE
POiMT
KL'VEER
$ ( '
i
3
^
(3> i
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1
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CL
SMtPLUiG
I»'i.««i
7
"/
2./
T-£
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CAS rETER REASIN:
(V.I. It3
KlITIfU: ( (
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SETTING ^i-1-5
/.(•
RECORD ALL DATA EVERY ^ MINUTES
ORIFICE PRESSURE
DIFFERENTIAL
imi. u. NjOl
DESIRED
lt(
/•(
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/, f?
ll$~
t.^r
t<*e
I.HO
ACTUAL
(<•(
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lt $
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7<9
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6 7
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PITOT NUMBER
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COMMENTS
no* .oicm !>*&<
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tro/{ O.O^CFH 6 " fjf
-\
-=^=*-_^,. „, ^_ ,. _ ^— -„„ , _ ' --^^-^X,^. '
TRAVERSE
PO;.IT
CLOCK TI.VE
SWPLIKG (24 lu
CAS f.ETEfl EEAOWG
(V.I. It1
VELOCITY
HEAD
ORIFICE PSES'.'JRE
OIFFESE.lt!>!.
STACK
TFJJ?ERATURE
ORYCASKETER
TE.T.»ERATURE
f\n?
VACUa.
IFKPERATtlRE
%
TRAVERSE
PO;.IT
SU.VBER
Clt
A.«PLIKC
TIV£,iti.i
CK TI.VE
i;
-------
-166-
MOISTURE
HPINGERS
FINAL VOLUKE
INITIAL VOLUME
NET VOLUME
ANALYTICAL DATA BY
SILICA GEL
FIMAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
TOTAL MOISTURE
ACETONE FRONT WASH
FINAL 95- ^/T 22"
TARE SS".q4-l.-)
NET 3 !.?'
FILTER NUMBER 1
FINAL 3 COMK CASHIER H,
KYSEIF UVTIL DELIVERY TO A LASCRATCRI
F08 AMLtSIS.
S1G^ED
WITNESS
OATE
DATE
DESCPI3EO BI1 THIS CATA SHEET FROM THE
A5GVE W£D INDIVSDUiL ATiD ;HfiLi2t3
This IK A:CCBDA»CE VIIH IKE ABOVE
NAU-D PROCED'JP:.
SCCTT ENVIRONMENTAL TECHNOLOGY, INC.
SIGHED
DATE
NOMOGRAPH DATA BY
CALIBRATED PRESSURE DIFFERENTIAL. ACROSS
ORIFICE. «u KjO
•YERACE rETER TESyERATURE (A.OTENT * S*F).'F
PERCENT tBIJTU'iE ;:< GAS STREW BY VOLUY.E
BAROMETRIC fRESSIME AT rETER. in. H(
JTATIC PRESSURE IN STACK, in. H|
f.i|.07J 1 STACK CAUCt FR'SUBE i» ». HjO)
RATIO OF STATIC PRESSURE TO «HER PRESSURE
AVERAGE STACK TESPEP.ATURE. *F
AVERAGE VELOCITY HEAD. ;». HjO
KAXiKUN! VELOCITY HEAD. in. KjO
C FACTOR
CALCULATED NOZZLE DIAV.E1ER. in.
ACTUAL KOZZLE CIA,"EIER. in.
REFERENCE i). in. H;0
4B,
'•„.
\,
'.
%
"'/P.
Tw
4'j,(.
4 'ML
DRY MOLECULAR WEIGHT DETERMINATION BY
SAKPLISG TIME (24-hf CLOCK)
SAMPLING LOCATION
SAI.iPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD
M5BIENT TEMPERATURE
^^ miu
\.«"N
GAS ^\
C02
(ty.icT is A:TU*L Oj
REWI.% 5l»!iS ACTUAL
CO;fiMOllS|
COlKTlSACIWlCO
Oj REAOINQ
ACTUAL CO RCAC1NQ
ACrtliL
PCAOIHC
SET
ACTUAL
«£7
ACTUAL
KAOiSC
BET
AVERAGE
litT
VW.WE
:'r:-f-:-'f|"i3r-'.:
.~-:n::ih:ii:ir::
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....
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col+J
h- U
a: aj
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0.1-p-
~o
*£\ QJ
O 4-»
-------
#2701-01-0280 -167-
APPENDIX C
PARTICLE SIZE
FIELD DATA SHEETS
Scott Environmental Technology Inc.
-------
-168-
AKDERSEN STACK SAMPLER DATA
f
Test/Run Number: /
Operator: \j
-------
-169-
ANDERSEK STACK SAMPLER DATA
Xti
, / 3 - / 9 7 9
Test/Run Number:
Operator: f\ j.. c..
Grain-Loading- From—li
Meter Box Nc. fByJU»..£> &AHa|.ST7 Andersen No. __
Nozzle Size ,
dscf
Est. Sampling Time 20 min.
Sampling Location & Point Number: Outlet/Inlet; Point j.3
Average Velocity Head
From H2 Traverse, APS
Average Stack Temp.
From H2 Traverse, Ts L'l
Flow Setting From Nomograph, AH /, 3 ___ Reference AP
Start Stop ^r> Elapsed_
Time : __ 7 ', a "5 'nn -- aM
ds cf/min
ECD
(Microns)
3
A
5
6
7
8
Back-Up
Filter
, \2- A-'/-
SCOU ENVIRONMENTAL TECHNOLOGY, INC.
-------
-170-
ANDERSEN STACK SAMPLER DATA
Date: ?t-v-. /3-/?7?
Test/Run Number:
Operator:
Meter Box No. HfiVA?,.., 6U->AHa |. p7 Andersen No.
Nozzle Size
Grain-Loading—Froa -It—5-
gr/
dscf
Est. Sampling Time
tnin.
Sampling Location & Point Number: Outlet/Inlet; Point 3' PC
Average Velocity Head
From 12 Traverse, APS
Average Stack Temp.
From 12 Traverse, Ts
:etting From
Nomograph, AH
Start
/o;i
Oof/l
/• 3
Stop
\0'£o P.tf
Reference AP £?.%-
Elapsed
A o
In
lain.
Out A
Time:
Gas Volume: Final
Initial
Meter Temp: Final
Initial
i / / gi f, ^
Total / I , I £ cf.
Stack Velocity Head, APS
Flow Rate, All
Stack Temp, Ts
i .lb/
Ib-mole
Gorrected-Volume
dscf Gorree-ted -Flow- Ra te-
dscf /min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g)
Net (mg)
Cum. %
BCD
(Microns)
\2-S.O
3
4
5
6
7
8
Back-Up
Filter
\4OC?
1 2- 5.0
O.I
SCOn ENVIRONMENTAl TECHNOLOGY, INC.
-------
Date: //-/?- 7
Operator: fr] rT ~ B I?. Meter Box No. J
gr/
-171-
ANDERSEN STACK SAMPLER DATA
" Test/Run Number:
A ~
L
&AHa 11 7VZ) Andersen No.
Nozzle Size
Grain-Load ing -From -fi -5-
dscf
Est. Sampling Time
Sampling Location & Point Number: Outlet/Inlet; Point ^*-3 P$f\T A
ir.in.
Average Velocity Head
From 112 Traverse, APS
Flow Setting From Nomograph, AH
Start
Time: " H,'£O
Average Stack Teap.
From M2 Traverse, Ts _
Reference AP. ,
Stop
Elapsed
3 Q
Gas Volume: Final "2- 5~%-
Initial
In
Meter Temp: Final 110'
Initial
jnin.
Out
Total
Stack Velocity Head, APS
Koi-s-ture--From—?4~-f&) -
Cor retrted -Volume
Flow Rate, AH
Stack Temp, To
lb/"
lb-iaole
dscf
Gor-r-ee-ted—F-low-Ra-te-
dscf /min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
5
6
7
8
Back-Up
Filter
Tare (g) Final (g)
Net (mg)
%
Cum. %
ECD
(Microns)
V
, 14-Sr
, 1^01
l "5. 1 "?
1 •- >w >, fca«- w
0,0
SCOTT ENVIRONMENTAL TECHNOLOGY, INC.
-------
-172-
ANDERSEN STACK SAMPLER DATA
Date: I1 l3 ~ ?f Test/Run Number: ^ $ /-*. C,
\
Operator: ft~l\5~ BR Meter Box No. JSPLij' &AHa I'm Andersen No.
jG±J
gr/
G-r-a-in-Loading- Froirr-1i~5- dscf Est. Sampling Time / <^
Nozzle Size /
Sampling
Sampling Location & Point Number: Outlet/Inlet; Point"^ 3 pprfc~{
T •——-
Average .Velocity Head _^. • Average Stack Temp.
From fi2 Traverse, APS ' ^-^ From 1F2 Traverse, Ts
Flow Setting From Nomograph, AH I> V/; Reference AP-
Start ' Stop Elapsed
Time: "7/^0 2_1^ ]1 .nin-
In Out
Gas Volume: Final 3//|jjjT/'' cf. Meter Temp: Final //5~ "
Initial H^^_'^/^C^JL Initial /^/( ^^
Total ll'l/l1} cf.
Stack Velocity Head, A?s . 3 ST Flow Rate, AH // ^
-------
-173-
ANDERSEN STACK SAMPLER DATA
Date: / /- / 3"2
Operator:
Q
.
Meter Box
Test /Run Number:
&AHa l.
—.
/3
G-r-a-in~Load ing -
gr/
Andersen No.
Nozzle Size
dscf
Est. Sampling Time / f>
mm.
Sampling Location & Point Number: Outlet/Inlet; Point -3 y&f*
Average Velocity Head
From fi2 Traverse, APS
Average Stack Temp.
From .H2 Traverse, Ts
Time:
)mograph, AH
/ ' 7 (5 Reference AP ,3 j
:t Stop Elapsed
'0 J,2.-&S^ 1? min.
In Out A-<
iS-i.
Gas Volume: Final "*
"mf^ •*. r
Initial 3 //.JT9cf.
Total
Stack Velocity Head, AP
Mei-st-uire—From~^i4—(-%-)
Gorrec ted~VoluBie
Meter Temp: Final (I
Initial 7 &
7 7
Flow Rate, AH /.
/
•Ges-Dcn s-i-ty— F-r-e m— S-3-
Stack Tenp, Ts v g?
lb/lbHnoir~
dscf Gor-rec-t-ed-Flow—Ra-t-o
dscf /rain
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
2
3
5
6 ,
7 i
8 *}
Back-Up
Filter
Tare (g) Final (g)
v "S^-.S
I Z"?.O
I 3 (a)
Net (rag)
%
Cum. %
ECD
(Microns)
\-2b.Q
, 1380
SCOn ENVIRONMENTA!. TECHNOLOGY, INC.
-------
Date:
Ope r a t or : ~~\,
. r
-174-
ANDERSEN STACK SAMPLER DATA
Test/Run Number;
Meter Box No. ^Pf-W &AHa I .
Andersen No. -^
6ra-i-n~Loading--Frorr fi--5-
Nozzle Size. . I: *fe
Est. Sampling Time
mm.
Sampling Location & Point. Number: Outleti'/Inletj^Point
I- I
Average Velocity Head
Froia 112 Traverse, APS
Average Stack Temp. ^
From .??. Traverse, Is (g'tT.
Flow Setting From Nomograph, AH
Start •
Time: " \(
Reference AP
TStop_
I, <."£•
Elapsed
_min.
Out
Avc:.
Gas Volume: Final
Initial. 4?fr • °°° cfx
Total 1 *
Stack Velocity Head, APS
Meter Temp: Final
Initial
10?
Flow Rate, AH
Stack Temp, Ts
Moi-sl-ure- F-r-om-- ^4— (-%-) -Gas— Den8-i-ty-~Frem-~K-3< Md
Gorr ect.e d'-Vaiume d s c f Go r -r-e e t-ed-F-lo w- • Ra t-e-
lb/lb-,ole
dscf /min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (mg) % Cum. %
1
2
3
4
5
6
7
8
•7403 ,112.8 3^>^A'' \i1-b
.IZ5"-B »(^4^ \\\'
c*7 ' 4^3 Vi-£
, ^ s <^- * * » •-"
jzs-a , isn 5J x
\4-03 .•\ 0 • D
/
BCD
(Microns)
Back-Up "2.Q&.T O'O
Filter • XOvoTl '
v • ij.
f teOKJT" rO ^i tA ^4?*V\ Vit-"^— "
f^tkitVV &&» ^"^
14-
£} SCOn ENVIRONMENTAL TECHNOLOGY, INC. Ofcwev.e' . °^.'
-------
Date:
It
-175-
ANDERSEN STACK SAMPLER DATA
Test/Run Number:
'*
Operator:
-T,
Meter Box No. t^g>*da-- &AHa 1 n C~Andersen No.
Grain-Loading- From-H-5'
dscf
Sampling Location & Point Number: Outletyinle,
/.!
Nozzle Size , ( 94"
Est. Sampling Time (C"E>
*•* a, fto'R"
mm.
Average Velocity Head
From fi2 Traverse, APS
Average Stack Temp.
From -U2 Traverse, Ts
etting From Nomograph, AH 1 i <->
Start • Stop
1^4--o
Reference AP I i
Elapsed
\ -ST
In
15
min.
Out A
Time:
Gas Volume: Final
Initial
Meter Terap: Final
Initial | I "3
I OS"
• Total I I"
Stack Velocity Head, AP3
Moi-sture—From—^94—(•&)
eorrected-Vo-1-ume
cf.
Flow Rai;e, AH
— Densi-L-y— F-rein— M-3-
Stack Temp, Ts
lb/'
Ib-mole
dscf eor-i-«cted-Flo'rf-Ra.fc<»-
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3 *
Plate
1
2
3
4
5
6
7
8
Tare (g)
. \3fe2
Final (g)
Net (m?.)
Cum. %
ECD
(Microns)
, \
.>2/?£
Back-UP on 1-3
Filter '^W
SCOn ENVIRONMENTAL TECHNOLOGY, INC.
-------
Date:
-176-
ANDERSEN STACK SAMPLER DATA
Test/Run Number:
Operator:
Meter Box No .
&AHa I |"\ ^~Andersen No.
Grain -Loading—From-H—5-
dscf
Nozzle Size * ) ff t#
Est. Sampling Time j
Gor-reot-ed-i-low-Rafeo-
Stack Temp, Ts
lb/'
Ib-mole
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
5
6
7
6
Back-Up
Filter
tare (g) Final (g)
Net (ins)
%
Cum. %
ECD
(Microns)
a.
\ Z fc.
7-7
s
/
/
\273 -i376
M-
v^
SCOTT ENVIRONMENTAL TECHNOLOGY, IMC.
< ^VV( Pt (<^
-------
-177-
ANDERSEN STACK SAMPLER DATA
Date:
-------
Date: I!
-178-
ANDERSEN STACK SAMPLER DATA
Test/Run Number:
VI
Operator:
Grai-n-Load ing-From-fl-
Meter Box No. **£'
gr/
dscf
_.&AHa l.g"? Andersen No.
Nozzle Size
Est. Sampling Time
rain.
Sampling Location & Point Number: Outiec-^TfiletpToint
Average Velocity Head
From v2 Traverse, APS
Flow Setting From Nomograph, AH
Start •
Time:
Gas VoluBse: Final
Initial
Average Stack Temp.
Froa
-------
-179-
ANDERSEN STACK SAMPLER DATA
i -"
Date: II I I S ( T? . Test/Run Number: -i^^^^V ettd^l C>7-
Operator: >. t?M^K> Meter T.ox No. &AHa (.8"? Andersen No.
Nozzle Size
Grain-Loading- From-""1 ''
Flow Setting From Nomograph, AH ) \ ^^ . Reference A?
Start . Stop I
Time: • | D M *S' 1^*?$ |fc
mm.
llL. _2ut. _^-l8-
Gas Volume: Final ^tK>.4"49 cf- Meter Temp: Final 73-•
Initial 49!, 9l-£ cjv. Initial ^ &"?>
Total "60 L^ cf<
Stack Velocity Head, APS Flow Rate, AH Stack Tenp, Ts
Ho-i-s-t-ure-Frot!>-^f4—(%•) •G-a-s-.-Denui-tv.~F--ftH':i—V-3- M/i ' Ib-mole
Corrected-Volume _ __dsc.f Gor-rec-ted~Flow-Rafee- dscf/rnin
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
ECD
Plate Tare (g) UTiiLls! Net (mg) , % Cum. %
.ie>5>f , ;4O6 ^'"'
6
7
8 • IT-SB , \Z£^ 0'^
Back-Up «« AC ^r o *7 cr
Filter ' ^0-S.O » w..^a
SCOn ENVIRONMENTAL KECHNOIOGY, INC.
-------
Date:
-180-
ANDERSEN STACK SAMPLER DATA
" Test/Run Number:
Operator:
Meter Box No. -£&>rr ^>e. & &AHa ; ,ft-? Andersen No.
Nozzle Size
Grain-Load ing -From •-'it -5-
gr/
dscf
Est. Sampling Time
min.
~ — "
Sampling Location & Point Number: Outle^/Inle_tj^-Point L"gr '
Average Velocity Head
From ti2 Traverse, APS
. o 0>
Average Stack Temp.
From .112 Traverse, Ts __ 6-1
Flow Setting From Nomograph, AH \ <1
Start
Tine: r
(?'•>
Reference AP
Elapsed
rain.
In Out Avg.
Gas Volume: Final 6>£tT."7
c.f.
Meter Temp: Final \O^c
Initial / C>3
Total 1'
Stack Velocity Head, APS.
Koi-sture—F-rom—1i4— <$•)
Gorrected—Volv.sie
cf.
Flow Rate, AH
Stack Temp, Ts
•Gas—Bens-i-t-y—F-r-efn-~¥-3-
Ib-mole
dscf Go r r ee-tred-Flo^^-Ra-t-a-
dscf /min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
Tare (g) Final_ _(g)
. I ^ to-^
3 - 13^.8
5 ,
6 ,
7 .
8 ^ •
Back-Up
Filter
Net (rag)
1n>/
M^
%
Cum. %
ECD
(Microns)
, /
, I 1?
, \
/
0
>
.St.
scon ENVIRONMENTA;. TECHNOLOGY, INC.
-------
Date:
, /5"'/9*??'
-181-
ANDERSEN STACK SAMPLER DATA
Test/Run Number:
Operator: f\i C.
Meter Box No. f\ Jb.J$ &AHa /. 7oV Andersen No.
Nozzle Size
Grain-Load ing-Frora-fi—5-
gr/
dscf
Est. Sampling Time jQ. £>
rain.
Sampling Location & Point Number: Outlet/Inlet; Point f\
Average Velocity Head
From 512 Traverse, APS
Average Stack Temp.
From 112 Traverse, Ts
Flow Setting From Nomograph, AH
Start
Time: " 7
Reference AP
Stop
Elapsed
In
TO in,
Out
Gas Volume: Final ^ ( O.o2.cf.
Initial 3 g ?. 3Vcf,
_ ._ _.^-
Total 3v /. 4E cf.
Stack Velocity Head, APS
Meter Temp: Final £> 2,.' 6 Z.
Initial 6 0 d? O
6 0 x
Flow Rate, AH
Stack Teinp, Ta
•Gas—Dens i t-y--F-re!R—5-3-
'ib-molc
Corrected -Volume
dscf Gor-r-ec-ted -Flow~Ra-t-e-
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
5
6
1
8 ,
Back-Up
Filter
Tare (g) Final (g)
Lk
7
Net (mg)
Cum. %
ECD
(Microns)
3
b.O
*
SCOTr ENVIRONMEMTAl TECHNOLOGY, INC.
-------
-182-
ANDERSEN STACK SAMPLER DATA
Test/Rur Number:
Operator: A I- C - T"£-
Gr-a-in-Loading- From- *i~5'
Meter Box No. /? X.r...-ffi. &AHa /. 7 J^ Andersen No. 7
Nozzle Size ,. ^.
dscf __ Est. Sampling Time _. _ £f>
/
mn.
Sampling Location & Point Number: Outlet/Inlet; Point /•) ,3
Average Velocity Head
From 512 Traverse, APS
Setting From Nomograph, AH
Start
Time: / Q f 5$ ft ft
Average Stack Temp.
From 5)2 Traverse, Ts
Reference AP
Stop
/ f . Qt) fl
Elapsed
In
Out
AVP.
Gas Volume: Final
Initial ¥fe9..//
Meter Temp: Final
Initial
Total / /
Stack Velocity Head, APS-
liois-t-ure—From—M4™(%-)
e-or re c t. e d- -Vol-ume
Flow Rate, AH
Stack Temp, Ts
-Gas—Dene-i fry~-F-i.-CMVt~'i 3-
d s c f Gor-ree-ted—F-lcw--Ra£e--
Ib-mole
dscf /min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
6
7
8
Back-Up
Filter
Tar^_(g)_ Final (g)
.no
Net (rag)
%
Cum. %
ECD
(Microns)
, 1 *2.iP.\
\\'\
o
.1
•i scon ENVIRONMENTAL: TECHNOLOGY, INC. .
-------
Date:
-183-
ANDERSEN STnCK SAMPLER DATA
Test/Run Number:
Operator: flic - J
Grain-Loading- From -fi
Meter Box No. AJ^.tfC &AHa/,70y Andersen No. ^I/V^
Nozzle Size , 2So
_dsc_f Est. Sampling Time <7~ min.
Sampling Location & Point Number: Outlet/Inlet; Point
Average Velocity Head
From fi2 Traverse, APS
Flow Setting From Nomograph, AH
Start •
Time :
Average Stack Temp.
From .1)2 Traverse, Ts (, 7 °p
Reference AP. M¥
Stop
[ .-...
Elapsed
Gas Volume: Final
Initial
I .
In
Meter Temp: Final /Ob'
Initial / Mj
d s c f Go r r ee-Ued-F low-Rate-
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (rag) __J>
Cum. %
2
3
A
6
7
8
Back-Up
Filter
b
o:
Stack Tc-Kp, Ts
Ib-mole
dscf/min
BCD
(Microns)
SCOn ENVIRONMENTAL TF.CHMOLOGY, IHC.
-------
-184-
ANDERSEK STACK SAMPLER DATA
y
Date:
II n
Operator:
6rai-n~Loadin2~From-?
Test/Run Number:
Keter Box No. 5<&M~_^'__ &AHa ( S&* Andersen No. _(
8r/dscf
Nozzle Size ,
Est. Sampling Time
min.
Sampling Location & Point Number: Outlet/Inlet; Point
*-? -s-t.
Average Velocity Head
Frojfl 112 Traverse, APS
Flow Setting From Nomograph, AH ___
_Start
Tirae: / J
Average Stack Temp.
From 12 Traverse, Ts _ ^ ~7
I. * S"
hrf_. Reference AP / 2- 1
Sto
Elapsed
~
In
jnin.
Out
Avg.
Gas Volume: Final /#2/,
Initial 9 3" 7, 3^g cf.
cf.
Meter Temp: Final
Initial
Total
Stack Velocity Head, APS
Moi-stur e-Frotn- -C.14- <-%-)
Flow Rate, AH l
•Ga-s—ben-a-i-fey—F-rom
Stack Temp. To ^ ~7
c f *3 ^CC»-I_ -.-
lb-mole
dsc f Goi-ree-'i-ed—F-low—Ra-te»
Temperj'.ture Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
5
6
7
8
Back-Up
Filter
Tare (g) Final (g) Net (tng)
%
Cum. %
dscf/rain
BCD
(Micror.s)
o
tOASrt ,
£4.
SCOn ENYIROHMENTAl TECHNOLOGY, INC.
-------
-185-
ANDERSEN STACK SAMPLER DATA
Date; /•/«rtC>
Operator: jnj±t_ Meter Box No. _£>_o*»fr &AHa _/.J??_ Andersen No. 'i:r' /'-/ '•'.•?
Nozzle Size . 0 17)
, r^.1
Grain-Load ing- From -iHr b dscf Est. Sampling Time join.
Sampling Location & Point Number: Outlet/Inlet; Point /?,.*\ <• / ••- "*•> V^-u U
Average Velocity Head Average Stack Temp.
Fro;a ^2 Traverse, APS /_/ 2-^ From .fi2 Traverse, Ts ~) $?
Flow Setting From Nomograph, AH ^ .V Reference AP- , 9~';
Klapsed
ime : __ A££:_'. _______________ I $~O f? ___________________ 1. ' V ______ >«in .
/ r ^5- // f>f* • / 3 -5"5" /^ /Q /£r7.
Gas Volume: Final 7V ^. 76 ^cf. Meter Tern?: Final P# 7 & ^
linitial ?c,^ ^^c/c^f . Initial 75^" 7 5~"
Total \^' r^1 cf.
Stack Velocity Head, APS ___ Flow Rate, AH _JLC/. ___ Stack Temp, Ts _7 X^ _______
~l:'rom-^4'-{yj-) -Gas-Dens-ity— F-rem-^-3- Mj Ib-rnole
C-oz-rcctsd-Vol-u'-ne _____ dscf Gor-rec-t-ed-Flow-Rat-a- _ _______ dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3 ____
ECD
Plate Tare (g) Final (g) Net (mg) '___% _ Curs. % (Microns)
" ~
2 . )Z ./ft 5V
3
4 ^p 139,9
5 ,
6 . _ .
Back-Up ,-?5f.»
Filter
SCCn ENVIRCNMENTAl TECHNOLOGY, INC.
-------
-186-
ANBERSEN STACK SAMPLER DATA
Test/Run Number:
Date: fis ffu<*t* jisr f 7 . 1^7^
-j ' jc,ti/-4*s& r~~b~~/~~
Operator: /5 9 < \ Meter Box No. /'5v>-'' /> &AHa /e f 7 Andersen No. 'jf/.i^.;—.
*-—i. f
8r/,
yr-e-in-Load ing- -From- H— 5-
dscf
Nozzle Size _."}._/ /y ''
Est. Sampling Time j' £? '
roin.
Sampling Location & Point Number: Outlet/^nlep, Point /^}? .5 J~d-/^Sf 3
Average Velocity Head
From fi2 Traverse, APS
Flow Setting From Nomograph, AH _^_
Start
Time:
Gas Volume: Final 7 ?
Initial . 7j
Average. Stack Temp.
From -U2 Traverse, Ts
Reference AP. >
Stop
Elapsed
In
jnin.
Out
Avjr.
Meter Temp: Final ~? &
Initial y ^
Total 0
Stack Velocity Head, APS
Mo-i.-s t-ure—Frora—V-41—{-%•)
Gorrected-Vcrluaie
Flow Rate, AH
•GaS'-Dens-i-t-y— F-renj—^
Stack Temp, Ts _7_V_
lb/lb-mole
dscf Cor rec-t-ed-F-low-Ra-fee-
dac f /min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3 i
4 •
5 ,
6 .
Tare__(gJ>_ Final (g)
.2.31,5"
Net 6ng")
%
Cum. %
BCD
(Microns)
VI
lo.
y
Back-Up ^ . -I
Filter L I /,i
\ '
SCOn ENVIROKMENTAL TECHNOLOGY, INC.
-------
Date;
- 7?
Operator: />1
Grain-Load ing—From -1i—5-
-187-
ANDERSEN STACK SAMPLER DATA
• Test/Run Number:
Meter Box Ko./^QV &AHa
gr/dscf
Andersen No.
Nozzle Size , 2.5? &
Est. Sampling Time
mm.
Sampling Location & Point Number: Outlet/Ra t-e-
dscf /min
Terr.perature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
2
3
5
6 •
7 '
8 '
Back-Up n
Filter ' /-' •$ i>
Tare (g) Final (g)
Net (mg)
' 3^;
%
Cum. %
• ECD
(Microns)
35-4'
1-1
1.1-
H
SCOn ENVIRONMENT/1 TECHNOLOGY, INC.
-------
Date:
Operator: /;
c>
Grain-Load ing
-183-
ANDERSEN STACK SAMPLER DATA
Test/Run Number:
Meter Box No.,/* 7£>y &AHa
gr/dscf
Andersen No.
Nozzle Size
Est. Sampling Time
min.
Sampling Location & Point Number: Outlet/^n^e};; Point >' '-•>£. K L~&£**.{,
ft~^ '
Average Velocity Head / / Average Stack Temp.
From *2 Traverse, APS \ From .12 Traverse, Ts (0&>
I ) SI
Reference AP 0
.„/,., ^ -~ /
Flow Setting From Nomograph, AH _ _J_' <^"_
Start Stoj:
Time:
Elapsed
In
mm.
Out
Avg.
Gas Volume: Final
Meter Temp: Final
Initial
Total ^^cf.
Stack Velocity Head, APS.
Flow Rate, AH
•Ga-9—Dens-i-vy- •?•
St ack Temp. Ts
ib/'
lb-raole
Gorrected" Volume
dscf
Gor- r-ec-ted-Flow-Ra U
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
5
6
7
8
Back-Up
Filter
Tare (g) Final (g)
V
Net (mg)'
Cum. %
BCD
(Microns)
* ^n =- 5^,1
\372.
Z
IZ7.D
o^
c.'i
/
7,1*7?
o-o
SCOn ENVIRONMENTAL TECHNOLOGY, INC.
-------
#2701-01-0280
-189-
APPENDIX D
VISIBLE EMISSIONS
FIELD DATA SHEETS
Scott Environmental Technology Inc.
-------
Sec
Mir.
X*
o
0
1-
2
R
6
7
__y
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A_2
13
14
15
30
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0
15
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18
Ua i/tr,
2.0
19 i /r/
20 ' —"•
21
22
23
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_25_
26
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28
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Sec
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30
_3A
_33_
34
35
36
15 j 30
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45
-JA\
T P - '
PLUM!'. OBSERVATION DATA
Run No. ____ / _______ Date__/lLL3_L2_2_
_zr.
J-O
t
JLQ
«4£._.
—t
3 P.
_39_
40 I //
4JL. [ _.[_y.. \ ( x_
\MLLtJ-\Jl \J-t\
LQ_
_1L_! i
i--
_/(l
44
Loca t ion
1 7^7
~\—\
T'T T>ir> TXe*T -i
L J Lit." i)1^..^.!.
Stack He!
Distance to Stack
Wind Direction
Speed
L J Sky Description I ™ VUU f
^ -. __.-
-1
Sum of Readings
i
t—*
o
_45_
46
_48_
AL.
50
Iijj T0ta3 No. of Readings
| ! ] i ' ~~~::~ ~~
Opacity = -\"— — ~—-^4^S^
No. of Rea^To.fs
51
52
53
56
58
~r~
(._
5U
__5L I L L i j
xrSTT"
.->••-
....__! i
^T5.--A.^i,/Hi I;!
Environmental Technology
-------
e
ts\
?v
§
i. •
§
3
n
rr
-V
v<
8
Sec
Min
0
2
3
. 4
5
6
7
, 8
9
10
11
12
13
14
15
16
17
18'
19
20
21
22
23
24
25
2.6
27
28
V
29 '
0
(0
". . —
/3
/ t~~
1-0
Id
I A
I 0
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10
10
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to
to-
10
10
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10
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30
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L u
LQ
id
ta
y
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10
10
10
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[6
16
10
fO
/Q
1 c"~^
10
if
10
IV
0
=s^r
— 35^
•=^=-
==yrr
Sec
Min
30
31
32
33
34
35
36
37
38
39
4 OX
41
42
1 43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
0
I15
i —
30
45
.
i ' • e^-vr- «— »
PLUME OBSERVATION DATA
Run No. 1 Date //— /"S-7^ Proj .//^"^(J [
Plant C^P/tCzS $ J^/h^D/hS
Location(//?]A/)fi-/(y£jS(j£tf.£-?t T^iS'^T i. ~r~o T>&^ 2.
r\ -
Observer fli fc ' C(f^\ /\ fj-
Time Begin [ (j Q "^ End ((f 3 6"
Stack Height ^Y^~ £.£V£r1_-
/
Distance to Stack /$
Wind Direction Speed
Sky Description lW£>0(J)t
kl6(i~r L&V&L, Lo o,V
( h— *
Sum of Readings '-'
Total No. of Readings
Opacity - |-um ofc Readings
No. of Readings
•
=
F""'".-";.t> '.' " ''4 f'^^^\ fi r^
If''' ^Rr llj ^"^ i "!j ^ ^ } t j ^1
fj^X . V' -''£'"' vj ^•^^•"^l/'\i!'''lij^H^""'',S' iiihj Vj^"
K "{fr^'''?^ " ^=i»~* >L^r*i«^ ^4^. — ^
irs- .^f'!'':i:», i^5 Fnvirnnmental ! r>ohnoloQy
r- *7
-------
Sec
Min
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
0
15
30
45
•
Sec
Min
30
31
32
33
34
35
36
37
38
39
40
4.1
42
43
44
45
46
47
48
49
50
• 51
52
53
54
55
56
57
58
59
0
15
30
f
45
Run No.
Plant
Ob s erver /) , P .
Time Begin
PLUME OBSERVATION DATA
Date//-/3 ~ 7 7 Proj.// 2-7 O (
73^-.. . „_._.
^<
-_A
End
Stack Height
Distance to Stack //"'
Wind Direction
Speed
Sky Description
Sum of Readings
Total No. of Readings
Opacity = |HI!Lpf
ings
No. of Readings
Environmental Technology
-------
(to
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*$*
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tal Technology Inc
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30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
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Plant
PLUME OBSERVATION DATA
Date jj
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Min
0
1
2
3
4
5
6
7
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9
10
11
12
13
14
15
16
17
18 '
19
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22
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PLUME OBSERVATION DATA
Run No.j£.
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0
1
2
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5
6
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9
10
11
12
13
14
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30
31
32
33
34
35
36
37
38
39
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41
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1
2
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6
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10
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12
13
14
15
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Accumulated
Emission
Time
(Min: Sec)
/ 7 :
-------
FUGITIVE Ef, ^ '' ^.- lJ ^ D AJ r\
Company Rep. J?L ft- /"£ 'A/^dc?
Sky Conditions '
Industry />-) &TTS1 1- L < ' <- s~**>££-'
*
Inspector /h j4-*,-j-\s *4 % ^ -jh*-X A, ^-7"T /rk^y/JP^K^-^f-^^i
Date /l'/^"n
Wind Direction A ^ S /
Wind Speed o - 5^,* .//'
r
Process Unit C^/lj.f^ C'^,,> '.^l/:.*--
"Sketch process unit, indicate observer position relative to source and sun; indicate potential emission points ar.d.'o"
actual emission points.
OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(iVIin: Sec)
Accumulated
Emission
Time
(Win: Sec)
, a
2-T> 2.7
-------
-259-
FUGITIVE EMiSSiON INSPECTION
OUTDOOR LOCATION
Company CYPRUS
Location
r""*» . i i'1''* , -' *
Company Rep. r'-'^'-X/'J' -^Xfb-M*
Inspector
Affiliation *
Date //~/JT"?9
Sky Conditions
Precipitation
Wind Direction
Wind Speed t
Industry
Process Unit
"Sketch process unit, indicate observer position relative to source and sun; indicate potential emission points ar.ci/ol
actual emission points.
OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(Min: Sec)
Accumulated
Emission
Time
(Min: Sec)
11 toy
-------
-260- :
FUGITIVE EfvittSfON INSPECTION
OUTDOOR LOCATION
7
Company O v / ^ ,- 0 «, iba^^fl- Cs-^nfs f~ .<*>
/^ / y / ."
Location /-/ i / 1 .*>': J f.- L-0 ]A d & '&T ~Co /U 'L/dV&f^
Company Rep.
• Sky Conditions ^*. [e.^f.
Precipitation
Industry /VlevW/., <^>^
'
Inspector A^ 3"2?/) M^Jo/v^
Affiliation c^ r ,?? /--y- >£>) i>/V^-"» "•'^A^S/
Date A//? tS r >* l> e. •* / & I *??$
Wind Direction A"^ / -f /v £ o 5 -f '
Wind Speed £T' •/'^ /
-------
-261-
FUGITIVE EMISSION INSPECTION
OUTDOOR LOCATION
Company
Location
\
Company Rep.
•"inspector //") J*~/* >•'•.
<, . /
Affiliation •or-.^-f ~f~
Date }/~1~l
Sky Conditions
Precipitation _
Wind Direction
Wind Speed
Industry
Process Unit ^/?.-/r)
-------
-262- „
FUGITIVE EMISSION INSPECTION
OUTDOOR LOCATION
Company C-V/P^yS pfi-G-D^k
Location IsitfeJ r> O*T*
Company Rep.
• Sky Conditions C-Q&f**! ..
Precipitation ..-•-? a, <.--».-<: .
Industry
.
,, fl,/ •
Inspector // » >*v-/i^i^*<—.
Affiliation ^f-r f^t^T
Date //"•/">"')?
Wind Direction ^/\C?
Wind Speed r°'> !°" fJ /*>,•*„•£
. .
Process Unit /~j>f;& nut £_&&tfflv\&.
h^-£.
Sketch process unit, indicate observer position relative to source and sun; indicate potential emission points ar.dTor
actual emission points.
OBSERVATIONS
Begin Observation
'O
\,
' L
Clock
Time
Observation
Period
Duration
(Min: Sec)
Accumulated
Emission
Time
(Min: Sec)
/A
/I, 6
-------
-263- ^
FUGITIVE EMISSION INSPECTION
OUTDOOR LOCATION
Comoany C_N/P$US BAG- 0:4 D
loMtion' HlU^jkLf
Company Rep.
Sky Conditions C1 L-pfi$
precipitation &
'inspector x|. r/AQ. A/^f L.
Affiliation ^^(^T r\ K/i/i^o^^r/^i-
Date lij}(.,/->q
/ ' '
Wind Direction ^ , '
Wind Speed CosTr/"}. f)-^
j
Industry
Process Unit
"Skotch process unit, indicate observer position relative to source and sun; indicate potential emission points and,-
actual emission points.
* OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(Win: Sec)
Accumulated
Emission
Time
(Win: Sec)
_M!
7'/o
-------
-264-
FUGITIVE ECvTiSSrON INSPECTION
OUTDOOR LOCATION
Company
Location
let Q ' Pft' ^/oA:V-, r/f'&fr
Company Rep.
. Sky Conditions j,/o ! •"" /-/^,/i Q [/£/? C-A S
Precipitation ."Z-Lj^.^
industry
inspector
Affiliation
Date
Wind Direction A/ It/. -
_
Wind Speed _____ _ ^2z^^
l_C>:^
Process Unit
Sketch process unit, indicate observer position relative to source and sun; indicate poteruia'i emission, poir-ts £ir.ci-vv-'
actual emission points. .. •''•
OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(Min: Sec)
Accumulated
Emission
Time
(Min: Soc)
J
IT
TFT
-------
-265-
FUGITIVE EMiSSION INSPECTION
OUTDOOR LOCATION
jompany Cy/0/?^ /3A&0^/0 . . .
cation \^)Ll$.]<4<> A2.
::o i n pa n v R e p. [A/ A to ^ f U
5ky Conditions ^C^j^t'^d-^--^'"'"'1'''" O^V-A,<),T7
;-»cipitation . ( >
J~f1~/()P PX '• '^''^Q Ol/tP^C.^^T^a^di'i'/lAT C'XlS^
iPJ'jstry ( 'o^A0/ ' ^'VW^ /| / jv,...
t.
^Inspector ^ /tfftQ/ /l/^-^L
Affiliation ^doT'T fzMl/lfthm-e yCT^j.
Date /V/7 /?q .
Wind Direction •§?£.
Wind Speed (^j? - $ >vii^^
'cl
Process Unit d//Q / /, ' /0/0c/ '< ^~ I^O(.^.
^
tch process ur.it, indicate observer position relative to source and sun; indicate potential emission points ar.c.
ja! emission points.
SER VAT IONS
'""- • } ' &,\\ f c,lv /Ts^> 5-* •
jin Observatio"n '' ^^^ ,
•
Clock
Time
&;<**
^;o^ ~ 1 r-Pc*
Observation
Period
Duration
.(Min: Sec)
00/v,n
Acc'jmtilated
Emission
Time "
(Win: Sec)
H'Sf
TD
'-}%'> L
-------
#2701-01-0280 • _256-
APPENDIX E
EQUIPMENT CALIBRATIONS
AND
SMOKE READER CERTIFICATIONS
Scott Environmental Technology Inc.
-------
STACK SAMPLER CALlSKATICtf SHEET
v.267-
by
T- • j
.-f • " '.:-/;..
Eox No.
;ican Quick Connects
Punp Oil
Valves
N
Dry Test Meter. . I;. ."~i ' — ,'^^- ~^ (c 1 0
r.erso-eters
Ights
Buzzer
lectrical Check - Aaphanol
.
ariac
/'
-eak Check at 27" Eg.' - Leakage 0 t< 3 ?
Vacuum Gauge
//
. 0 K.
CFM
e^arks
ate
• Kan
^ .r.
Orifice
CT
w
CALIBRATION - ORIFICE AND METER
No.
IT,
" '
CT '
T7
W
OT
""d
avg.
Pb
Time,.
t
0.5
1.0
2.0
4.0
"7.-?-;.'
33
10
To"
6.0
10
s.o
Calculate Y & AH/3 at as a. 2.0
CFt. P. (T. avg. + 460)
+0.147)
460)
0.0634
+ 460)
P. (OT, + 460)
O Q
Tolerances
CF
w
= 0.99 - 1.00 - 1.01
- 2.1
10
-------
.TlitttaMEj||itoBO.
Bo1
0.0317 (Man. orifice) /(T 4- 460)11 \2
if •*• i»
P, (OT, 4- AGO)
b a
CF
.Man.
0.01585
460)
AH,
CF P. (T. avf*. 4- 460)
w b u
CF
Man. _o r if Ice
."i3~*6 ' " (T 4- 460)
W
|.*VK£-
0.0317
0.0634
(
0.1268
0.1902
0.2536
>..T>J^
A.
0.0368)
4- 460)
V
l-ko.
+460)
../
.wi
0 4-460)
I L.o /.W
*60)\ 7. S'3^ /
^ X /
/(
4.0
A60)
% ^ a
•7—j—-~=—-v-"
/( ^6 4-460) 10 \2
Ul^l
1 3.
( ?£ 4-460) (6
,0 /.1SS6
x ,.
460)
.-l.Vb+ 0.0735)
460)
.^3-1 x 3.-I.;-n ( ^{7 + 460)
0.147)
460)
c \r-tr + 460)
0-29A) ( A fr + 460)
I 3.T-/0 x ^fl V/. ( | r. y 4 460)
0.441) ( (-0 + 460)
8,0 I.7&Y
/ 8
MxTrv^ju/uj:
15. ^3^. x M^' ( I fl 7 + A60)
/LJiLL A'1.-'^-*- 0.580) ( (fo. 4- 460)
Mun.
.5
1.0
2.0
4.0
8.0
-------
l'wii. tw.l
jLibraced by
K
n Quick Connects
^L
trhts
Lectrical Check - Amphenol
-269-
Box No.
-ak Check at 27" Eg.' - Leakage
sharks
Punp Oil n
Valves & /V
Dry Test Meter.
Buzzer
Vacuum Gauge
(rtJ
CFM
ate
CALIBRATION - ORIFICE AND METER
' Box No :
• Man
Orifice
CF
W
CF
T
A
Pb
avg.
0.5
60
1.0
2,
2.0
7 , l S-rO'T tv^Mn
-------
cALrinurriOFr~CALCULATIONS HETEK BOX CallSratedTy,
0.0317 (Man. orifice) /(T + 450) C \2 ' j
CF P, (T, avg. + A60)
w b d
Haa, orifice
P. (OT. + A60)
b d
0.0360) ( ££> + 460)
+A60) /O
0.294) (^ C + 460)
T-fr'37 ( f^/ + 460)
(3.9.37+ 0.441) (
rrcrrrj:»»**::.JJCWT/'.«.rJm . '•. IUBLJJHUII'JP .-
+460) /C> \
"
+ 0.588) (
-------
Calibrated by
Date
Clean Quick Connects
Manoceters '"' C
Themonecers
Light-
Electrical Check - Amphenol
\
Variac
STACK SAMPLER CALIBRATION SHEET
-271-
1
Box No.
Leak Check at 27" Hg.' - Leakage
Remarks '
Pump Oil
Valves
Dry Test Meter._
Buzzer
Vacuum Gauee
O K. -
CFM
Date
CALIBRATION - ORIFICE AND METER
Box No.
•• •-*•
• ' T
Man CF CF, TIT IT, OT, *d ' Pb Time.
- ,,. w d W d d t
Orifice avg.
V 0.5
1.0
2.0
A.O
6.0
8.0
/.^^
f f *'- .-
,-,.• . •v , ,-.
7.-M°?'.o
*. i" '
(,.-!!H'
. ^ r-. '
^ . } C-.':0
/ n i
/^ -~A ' "^
( . • /..:• J
'/.^<
i'.C,%
~>.0c/j'
r605-?
"-.-)
''o3
:'-. ';
^
'-. '}
'' ^ T>
si
/o'-s
/^'l
/r^
l\"6
\\^
^.^
•'-•'-. ^
(.7 T"
'.- -'.'
V (-
C-O
%
'• .' • i
?-'->
~~* r-~\
^ ;
/.•NO
•-^
c5c/.s'tT
r)C' ^<
^ q . <: //"
r'-°: "','*'
** \ *-• ^
; .»' ' * . ' .
-. •:, i ' '•
?' . •-> i
5
5
10
-10-
-10 '
10
Calculate Y & AH/g at man. 2.0
CF P (T, avg. + 460)
_ _ v b d
CF, (P, + 0.147)
d b
0.0634
, + 460)
(vv 4 460>
P, (OT. + 460)
D Q
CF
w
Tolerances
« 0.99 - 1.00 - 1.01
= 1.6 - 1.84 - 2.1
-------
CALIBRATION CALCULATIONS METER BOX Calibrated by \ • 'o'
Date 6" " oO '") °1 Box No.
0.0317 (Man. orifice
P. (OT, 4- 460)
b d
/
0.01585 N
&XV:V'( ^-^j 4- 460) I
. ~T • \
0.0317 /
I
^
0.0634 /
«0v ? •.*•>-('/<"" 4- 460)^
1
1 0.1268
,' "'/ •• ( " .<" + 460)
0.1902
__L2 ( I:';'.Q + 460)
^%
0.2536
! <-:'"' '' 1 ( ''") + 460)
s) /(T 4- 460)L \
j w
1
I CF» >
•
; 6>o + 460) v<
f
- .^o + 460) •-.:
/• • . '
k
(^o 4-460) .'.C
1 / ;.' '"' '
/( ,',o 4-460) •' '
1 ''"/I
\
^( .'..-:> 4-460) <
V ^!
f( f,-.-, 4-460) .<
, , i^
2 '
I
v
\
;
ft O
1
I
v\*^
1
/
%
1
|
/
•\2
J
\ 2
I i
/ '
Man i
_
i n
J. . U
2r»
. U
J_Llu_tD_
4.0
6rv
. U
«.»«.
i
8t\
'
i
@
/ . ' -=•..'•'
/.^I'6T
I :*'•*'* *
-
.
•
" '""" i
•
\.^5'/S
r
CF P. (T. avg. 4- 460)
w b a
Man. orifice
CF. (P. 4- 13.6 (T + 460)
d b w
..
/ . r. '.%\ X ,, .^ ^' ( .1 4" 460)
Ail/ U^T- 0.0368) (_^ + 460,
,;?..^?.^ x /)": i-/.> (J'l • + 460)
« •?""/'-'?' C'.O. :'"-*- 0.0735) ( '.% 4-460)
V 'i';.^. x ,?•'• ;' '.<' '( 7^ 4- 460)
"y.r'^1V(. ("•...< 4- 0.294) ( '-,o 4- 460)
C.TV| x' ?-'^-'.'-> ( /oo 4- 460)
7.C>c/( (."-'•'.'.: -'^4-. 0.441) (;' > 4- 460)
'/.V,-,x^.S7(/^A4-460)
(
fi.f><") <<1"i -.7+ 0.583) ( r..r> + 460)
Man.
.5
i n
7 n
4.0
6n
. u
o n
Y
t.oo~)f]
'.Col?.
/.^l,
-.oov.
-.our
I* -
I
IN3
—I
ro
-------
Calibrated by
Date
Clean Quick Connects
•Lanoneters
Ihemoneters
Lights
Electrical Check - Anphenol
STACK SAMPLER CALIBRATION SHEET
-273-
Box No.
13
Leak Check at 27" Hg. - Leakage
Eenarks
Pump Oil
Valves
Dry Test Meter. .
Buzzer
Vacuum Gauge
CFM
Date
CALIBRATION - ORIFICE AND METER
Sox No. /?/lC.
Man
f..f.
Orifice
CF
w
CF
tT
W
IT
OT
d
avg.
Pb
Time.
0.5
to
?7
fz
1.0
do
2.0
fc.Z
10
A.O
10
6.0
13.
to
A>£
10
8.0
10
Calculate Y & AH at man. 2.0
Y =
avg. + 460)
CF. (P. + 0.147) (TTT + 460)
d b W,
AH« =
Tolerances
0.0634
pb <°Td
i
+ 460) \
I
'(I
w
k
+ 460) V
^ .j
CF |
/
0.99 - 1.00 - 1.01
1.6 - 1.84 - 2.1
-------
.,.!.! ,;v\ I LOU C
CnLil.ruU'd by
0.0317 (Man. orifice) /(T + 460^ \2
CF P, (T. avg. + 460)
W D Cl
Man. orifice
CF, (P, +
do
13.6
(T -»• 460)
w
460)
( 3o./7 + 0.0368) ( L& +460)
460)
.%C ( 5?./7 + 0.0735) ( ^D + 460)
7 £33 x5A
+ 460)
(v3?./7 + 0.147) ( ^o + 460)
/o. 7Z/ x 3o./7 (7*^5" + ,460)
Go./? + 0.294) ( Lo + 460)
/3./IJ x ^V^ ( '77^+ 460)
+ 0.441)
460)
/V3./S x 30.1$ (/o:. b" + 460)
:lv9> (3Q / g + 0.588) ( bo + 460)
Man .
1.0
2.0
4.0
6.0
8.0
-------
I
I
7?
~275~
Barometric pressure, Pb = in. Hg
Dry gas meter I!o.
Orifice
manometer
setting,
AH,
in. H20
0.5
1.0
2.0
4.0
6.0
8.0
GAS volume
wet test
meter
YW. ^
ft3^
• . f.W!
5f.M|
ioiotfv
lOpoV-
10isov*
lOi^''
Gas volume
dry gas
meter
Vd.
ft3
X£%
Xlkg
IO,Zo\
/O.I 3 1
)0 J^
/d.uY
Temperature
Wet test
Meter
tfc/i
°F
—i **e 1
7* !rt
-7/Y*v
.-?f>iw
70*fa\
^/^
WA\<\
Dry gas meter
Inlet
^i'
°F
$2.
/$lpO
Time
e.
min
|) 'I7
li' 1 /
^'7^
/•W
^6L
7-4^
^•45
Average
Y
|,o,
1.50
1,01
\.J^
1.0^
M0>
1-oib
.. AH0
1-bb
Lit
\.1) -
M3-
\.S-
\-i-3
\-1^
Calculations
AH
CL5
1.0
2.0
4.0
6.0
8.0
AH
13.6
0.0368
0.0737
0.147
0.294
0.431
0.588
Y
Vw Pk (t,j + 460)
Vd(Pb * T&) (tv, + 460)
',MV 1 0- ^^
t't.t^ ! o, i°nff
ru^«^ ? I \ . o \ u7<
i-t -^i 1 \ , o "^ ^ V
U^1 ! l.oi^b
•J .'i') i 1 , 0 ? \ "b
AH9
0.0317 AH f(tw + 460) e]2
Pb (td + 460) |_ Vw
l.^S
(.1?^
I.7SI
l/Ub
j.g'l^l
U2'6
.
T = Ratio of accuracy of wet test meter to dry test meter. Tolerance = ± 0.01
« *
AH@ = Orifice pressure differential that gives 0.75 cfm of air at 70° F and 29.92
inches of mercury, in. ^0. Tolerance - ± 0.15
Figure 9. Suggested orifice and dry gas meter calibration and calculation form.
•*-
{
(
-------
Il "\\ " d^. 10 x r LJ CM.
KCUFKCL ft t'sacn co.
* 0 C IN U.S.A.
iU ••.:.:.:
lili! i:.
... „*-**-»-*_
I • » t f t ' :
MJH;!!;i!;!i]i-!iji!;hi!i!i!
^
<.)
I-0""1 i:;.i:!:
:::":;!;J-;;T; ;:;.
LiiJlIiUiiiJ
::i:i:l!;
'irnrn JT
•JiUiU,
jiilllij
'..r:!
.; l;;
MS
;!!.!jj!i!i!;i!iL;:i ;;;i|!i:: i-ii-:|jiHl:|ii!!!ii ij!i|!Jii
",'••> i'T't I"!7"! • • ? :'i •':' I'^IT
0
!!jip iij! if siiiitiij ii!; p^ijijiiiiii^!!! iiiijiiijitijiiiiiitjiiiijiij iiitttMiiiiiiifiiijiifjiiNifi
liilnniiiliillliliilliinin^lNiiliii; j^ll^iij^^
|lii|Sjp|^|$Q
W\i\i\
-iiii' :l!i
; I ;t
ilil
!!:!
'llilili
:ijl
ili-i
'i!!1
TIT! i i it j:: ru n i i j! • ITfnT:' TTil if; I
:; !::i;j:-i: ;:!::!•!!::•;I::::h;;:
l....,..,.i.... :...,...,.,.,. . ,i, ..i,
iyiliiiijliiiLlli: ljii!J:l LUill^lLaiJJjJl MLUJ
::jjl;:;i!:ii;;:,:'^:^:2ooiT;::,S/^;:;:f?y^Cf7^S'S^
11;'
!:H
Ml!
mmm
liri
;iii|i!ijlM!i!ii!i|jii!|;!fi !i;i]l|ii iiijjliii
iiiiiiililililiiirnliiliiiili!;;!!!!!!!!!!!!!]
Ul:
ij!!!l!i!
ilinii?;
!i.;-,'}!!;i
TiJE!Jlfrini!*
Hi!
liil
cir;r::
o:;
iiilMilii
iiii
rh-r
-------
-277-
Joe Wilson
VISIBLE EMISSION'S OBSERVER
QUALIFICATION RECORD
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15"
16
17
IS
19
20
21
22
23
2A
25
WHITE SMOKE
Actual
% , '
Opacity
95
15
. 55
30
30
20
15
20
tO
1*0
' 65
75
75 .
1+0
35
35
25
25
20
20
20 - .
20
30
30
60
Observer
Assigned
Opacity
100
75
50
30
25
20
15
20
ko
to
70
80
85
50
to
35
25
20
15
15
20
15'
to
. ^
15
Error
5
0
5
0 '
5
0
0
0
0
0
5
5
10
10
5
0
0
5
5
5
0
5
10
15
15
BLACK SMOKE
Actual
%
Opacity
95 '
95
80
70
75
60
60
't5
• to
to
20
. 25
20
15
• '15
20
25
30
30
30
15
15
10
20
20
Observer
Assigned
Opacity
95
' 95
85
70
* 75
60
• 65
50
t5
. 35
20
25
20
15
20
Error
0
0
5
o •
0
0
5 '
5
5
5
0
0
0
0
5
25 | 5
15
15
20
20
15
10
10
10
10
10
15 •
10
10
0
5
0
10 -
10
Test Date
Remarks
9/28/79
Test Location SCOTT Er/IROITMEirTAL
TECHNOLOGY, INC,, Plu^sceaaviile, PA
Certified by: Joseph Wilson
Instructor
Daniel-F. FitzGerald
Division Manager
-------
-278-
Bruce R. Markley
VISIBLE EMISSION'S OBSERVER
QUALIFICATION RECORD
1
2
3
4
5
6
7
8
9
10
n
12
13
14
15
16
17
18
19
20
21
22
23
24
25
I-.TttTE SMOKE •
Actual
•7
to
Opacity
95
75
55
30
30
20
15
20
1»0
hO
65
. 75
T5
ho
35
35
25
25
20
. 20
20
20
30
' 30
Observer
Assigned
Opacity
90
75
50
35
30
25
15
20
35
tiO '
60
70
65
50
1*5
35
25
20
15
15
10
*
10
25
25
1
60 1 60
Error
5
0
5
5
0
5
0
0
15
0
5
5
10
•10
10
0
0
5
5
5
10
10
5
5
0
•
BLACK SMOKE
Actual
%
Opacity
80.
80
1*0
35
30
30
30
25
20
20
20 :
10
10
10
15
10
10
5
5
5
5
10
L
>
5
5
Observer
Assigned
Opacity
65
70
35
35
30
25
25
25
20
* 25
20
15
15
15
15
15
15
10
10
10
10
10
10
10
10
Error
15
10
5
0
0
5
5 .•
0
0
5
0
5
5
5
0
• 5
5
5
5
5
5
0
5
5
5
Test Date 9/23/79
Remarks
Certified by: Joserh Vilson,
Instructor
Test Location SCOTT Elf/IROIIMZNTAL
TECHNOLOGY, INC., Pluj-steadviile, PA
_Daniel F..JFit?.G_eraia_
Division Manager
-------
D. E. Cocbe
-279-
VISIBLE EMISSIONS OBSERVER
QUALIFICATION RECORD
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15"
16
17
18
19
20
21
22
23
24
25
WHITE SMOKE
Actual
Z
Opacity
95
90
85
' 80
75
TO
65
60
60
1*5
1*0
50
1*0
25
30
20
20
25
30
15
20
20
10
10
10
Observer
Assigned
Opacity
80
75
80
70
65
60
65
60
55
1*5 '
^5
55
35
30
25
20
25
20
20
20
25
15.
15
15
10
Er-ror
15
15
5
10 '
10
10
0
0
.5
0
5
5
5
• 5
5
0
5
5
10
5
5
5
5
5
0
BLACK SMOKE
Actual
%
Opacity
95 '
85'
85
80
65
60
60
55
' ^
ho
30 .
25
30
25
•20
30
30
15
10
10
5
5
f-
5
0
Observer
Assigned
Opacity
85
80
75
80
' 65
75
60
50
1*5
1*0
35
25
20
15
15
20
20
15
15
10
10
10
5
10
0
Error
10
5
10
0
0
15
0
5
0
0
5
0
10
10
5
10
10
0
5
0
5
5
0
5 •
0
Test Date
Remarks
9/20/T9
Test Location SCOTT Eir/IRO^^IT
TECHNOLOGY, INC., Plunsteadville, PA
Certified by: Joseph Wilson
Daniel F. FitzGerald
Instructor
Division Manager
-------
J. Marino
-280-
VISIBLE EMISSIONS OBSERVER
QUALIFICATION RECORD
1
WHITE SMOKE
Actual
%
Opacity
95
2 100
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22'
23
24
25
85
80
65
60
50
l$0
1»5
»*5
35
30
25
20
15
15
20
55
60
25
20
15
15
20
1*5
Observer
Assigned
Opacity
90
90 .
85
80
70
70 '
60
fee
liO
^5
30
25
20
20
. 20
20
30
1*5
55
30
15
15.
15
15
30
Error
5
10
0
0
5
10
10
0
5
0
5
5
5
0
5
5
10
10
5
5
5
0
0
5
15
,
BLACK SMOKE
Actual
%
Opacity
95
85'
85
80
65
60
60
55
>*5
1*0
30
25
30
25
20
30
30.
15
10
10
5
5
5
5
0
Observer
Assigned
Opacity
90
75
' 75
75
65
70
..60
55
' U5
50
30
35
35
'30
25
ho
35
20
20
20
20
10
15
10
10
Error
5
• 10
10
5
0
10
0
0 .
0
. 10
0
10
5
" 5'
5
10
5
5
10
10 -
15
5
10
5
10
Test Date
Remarks
9/26/79
Certified by: Joseph Wilson
Instructor
Test location SCOT? ETTVIEOriMEIJTAL
TECHNOLOGY, Il.'C., Plurjsteadville, PA
Dcniel F. FitzGerald
Division Manager
-------
Maynard Johnson
-281-
VISIBLE EMISSIONS OBSERVER
QUALIFICATION RECORD
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
WHITE SMOKE
Actual
%
Opacity
85
90
90
85
85
80
75
70
70
40
50
55
40
25
25
20
25
25
25
15
25
10
5
5
5
Observer
Assigned
Opacity
95
90
85
80
75
70
65
60
60
45
40
. 50
40
25
30
20
20
25
30
15
20
20
10
10
10
Error
10
0
5
5
10
.10
10
10
10
5
10
5
0
0
5
0
0
0
5
0
5
10
5
5
5
<
BLACK SMOKE
Actual
%
Opacity
90
90
• 85
65
70
70
65
65
50
30
25
20
15
20
20
10
10
15
10
10
10
5
5
5
5
Observer
Assigned
Opacity
95
85
80
60
65
70
75
70
50
30
35
20
15
25
15
10
15
15
10
15
10
15
10
5
5
Error
5
5
5
5
5
0
10
5
0
0
10
0
0
5
5
0
5
0
0
5.
0
10
5
0
0
Test Date
Remarks
9/20/79
Test Location SCOTT ENVIRONMENTAL
TECHNOLOGY, INC., Plurasteadville, 'PA
Certified by: Joseph Wilson
Instructor
Daniel J. FitzGerald
Division Manager
-------
From.
•7^
STATE OF CALIFORNIA
AIR RESOURCES BOARD
This Certifies That
.ITM
Has Attended The
VISIBLE EMISSION EVALUATION COURSE
OCTOBER 16
.to
OCTOBER 15, .197?
Chief, Division of Legal Affairs and Enforcement
w*
vm
i
wfi
ryvry
*&&l
fj\fi
&£>
$&
W
ttft
Clitcf, Enforcement Branch
CO
1X3
I
-------
-283-
APPENDIX F
TRACE ELEMENT ANALYSIS
Legend:
Sample #37689 - Not Applicable
Sample #37691 - Not Applicable
Sample #37692 - Secondary Crusher Scrubber
Inlet, Run 6
Sample #37693 - Conveyor Exhaust, Run 9
Scott Environmental "technology Inc
-------
-284--
CASLE ADDRESS "LUDO'JX TEANECK1
TELEX 134340
No. !PJL4-2k5_
359 Alfred Avenue, Teaneck. New Jersey 07666 • Telephone: 2/2 W7^j
} liVOm.SClE.VT COMROl.A.'.D P.?.?.: AftCH CriEM'STRY. l.aii7RUM = fiTAL AND CHEMICAL ASAlYjiS • SAMPLING.
ACS, f V<£ICH!?1G. SHIPPERS' RE?SE5£;irAT!CN, SEficflCIATIO'l. AND STOflACE OF OIIES AND METALS
r/W-
REPORT OF ANALYSIS
October 31, 1980
Our analysis of the sample of Dust Samples
From York Research Corporation
Marked: 15 lots as below: P.O. #3-5830
and
submitted to
us, shows:
•••; -•--. PARTS' PER MILLION -
-• .^3769.1 #3 7 6 92 #37693
•"-- -URANIUM '• —-——.: -<1. •-
THORIUM "• •» •— •— — «—• •—• AA \J f
,'"•"' "^THALLIUM -—— "<1.
'""• "MERCURY -„--_-—-_—„' <20
GOLD — <1.
PLATINUM <20
IRIDIUM r- <10
OSMIUM <2a
RHENIUM <2e
TUNGSTEN <2,
TANTALUM — <1.
P"fiT?WTTIM — ~ ^9
Ii*. ii\_LW»i «•—.«- — V^i. ^
LUTETIUM '• <002
YTTERBIUM <1.
THULIUM <0.2
ERBIUM <1.
KOLMIUM <0e2
DYSPROSIUM
-------
-285-
CA3LK ADDRESS "Li-.r'OUX T.t^NECK"
TliLEX 134340
/J^ 359 Alfred Aven\ie,.Teanect:. New Jc^cy 07666 • nh
No. yy^y " CONTINUED
l.'JCirtriUSNT COMf-.3l. A';0 RcSS.'.RCH CHEHISinv.lNSTr'.UN'EfiTAt AN3 CHEMICAL ANAIV;:; • S.V.»»LI."iS
wEIGKir.S. SH!??[H3' RtrH£SJf.:AllO,V. BEStriCIAIIO1.'. tr.D STOr,.\GE OF CRE^ /1'jU MJTALS
REPORT OF ANALYSE
Our analysis of the sample of Dust Samples
From York Research Corporation
Marked: 15 Lots as below: P.O. #3-5830
and submitted to us,shows:
PARTS PER MILLION
rFpTTITI
T AFTHAMTIM _
RAPTTJi.-J
pTT C T T f P^
• inTVi i>-'F -
TFTJTTRTITM - --
AHTTMOMY
TI>T - -
TMDTTJf" -
97TVFR --
PALLADIUM
Tr?TT...r
MOT.YBDFNUM -
NIOBIUM -
7 T "P ^ O M T I f f"^
vrr,,_^ ' il
'STRONTIUM -
RUBIDIUM
BPOMIrF --
o TTT FMTUU - -«-
ARSF'ir -
OFRMAMTTTM -
7.TKFH —
Lots #37689
_ __ i nn
JLUUc
snn
JUVJ c
— — 1
le
— .- C
5.
i nn
1UU,
X
. <0.5
i r\c\
^r\
<20
CA
To York Research Corporation
- . v(Page 2 of 12 Pages)
LEDOUX & COMPANY
-------
•1 f.'.. -?t ffl; a .-<
EST. ItSO ^ S*
-286-
CAPL.E ADDRESS "LEDOUX. T£ANECK"
TCLCX 134340
No. !_QU2l_5_
>«&:.& # 9 '•* '^£'" ^ !lt*'"'«•*. 7«H!e<*. AW /me;' 0 7666 . Telephones: 20( s* 7 716_°
•j \^j tit. 9-i 7 09^3
J INDEPENDENT CONTROL ANC r.f SEARCH CHEMISTRY. INSTRl'MtUrAl. ASO CHEMICAL ANALYSIS • SAVPllNI
A, S0 f WEIGHING. SHIPPERS' REPHJSCNTATIO.N. BcKif ICIAT1G.S. A.VO STOHAGE OF ORES AND METALS
REPORT OF ANALYSIS
October 31, 198.0
Oar analysis of the sample of Dust Samples
From York Research Corporation
Marked: 15 Lots as below: P.O.'#3-5830
' • •PARTS PER MILLION
and • submitted to
us, shows:
pnp^T^p
\7Tr"/^r, _ _
COPA* T
T-p^M ^ _ _
MAVOfl iVF>F
CFPO^TUM -~ -
VAMArlTiTM _
r?TrT1AMTITr.T _ _
9P4NPirr?.T -
PO^ASSTffV _
pUTf)r3T7\7p
SULFUR - - - -
PHOSPHORUS - --
^ILTCON -
ALUT'"I'-TT]?4
I^AGNF^TUr'1
SOHTIIM _ _ _ _
FT Iin^TMF _
pfii?ar)M _
RQ^ON
BFRYLLIUM
LTTHTKi.-!
Lots #37689
c$0
trnn
,)UU«
20 0
son
A
t\
M
9nn
------- |