United States
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park NC 27711
EMB Report 80-MET-8
May 1980
Air
Metallic Minerals
Emission Test Report
Union Carbide
Hot Springs, Arkansas
-------
FINAL REPORT
2705-01-0380
Emission Test Report
Vanadium Ore Processing
Union Carbide
Hot Springs, Arkansas
EMB Report No. 80-MET-8
EPA Contract No. 68-02-2813
Work Assignment Mo.
Prepared For
Environmental Protection Agency
Emission Measurement Branch
ESED, Mail Drop #13
Research Triangle Park, N.C. 27711
March 14, 1980
by
SCOTT ENVIRONMENTAL TECHNOLOGY, INC,
2600 Cajon Boulevard
* San Bernardino, California 92411
Scott Environmental Technology Inc.
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12705-01-0380
TABLE OF CONTENTS
Page Number
LIST OF FIGURES— i
LIST OF TABLES-- - — --— 11
1,0 INTRODUCTION • • 1
2,0 PROCESS DESCRIPTION 8
2.1 PROCESS SAMPLES 10
2.2 PROCESS OPERATION-COARSE ORE DRYER 10
2.3 PROCESS OPERATION-DRY GRINDING — 12
2.4 PROCESS OPERATION-COARSE ORE STORAGE BINS 13
3.0 SUMMARY AND DISCUSSION OF RESULTS 14
3.1 COARSE ORE DRIER--- — ~ 14
3.2 COARSE ORE STORAGE BINS — 37
3.3 COARSE ORE GRINDER 37
3.4 FINE ORE BIN AND TAILINGS POND 78
3.5 TRACE ELEMENT ANALYSIS 78
4.0 SAMPLING AND ANALYTICAL PROCEDURES — 86
4.1 SAMPLING PROCEDURES 86
4.1.1 SELECTION OF SAMPLING LOCATION-EPA METHOD #1 86
4.1.2 MEASUREMENT OF GAS VOLUME FLOW RATE-EPA METHOD #2—— 86
4,1.3 AVERAGE STACK GAS MOLECULAR WEIGHT-EPA METHOD #3 89
4.1.4 DETERMINATION OF STACK GAS MOISTURE CONTENT-EPA
METHOD #4— — 89
4.1.5 DETERMINATION OF PARTICULATE EMISSIONS-EPA
METHOD #5 — 89
4.1.6 DETERMINATION OF PARTICLE SIZE-ANDERSEN CASCADE
IMPACTOR —- 89
4.1.7 DETERMINATION OF VISIBLE EMISSIONS-EPA METHOD #9 89
4.1.8 DETERMINATION OF FUGITIVE EMISSIONS FROM MATERIAL
PROCESSING SOURCES——— 92
4.2 ANALYTICAL PROCEDURES—-- — 92
4.2.1 PARTICULATE EMISSIONS-EPA METHOD 15 92
4.2.2 PARTICULATE SIZE-ANDERSEN CASCADE IMPACTOR—— 92
Scott Environmental Techndosy Inc.
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#2705-01-0380
TABLE OF CONTENTS continued
PageNumber
APPENDIX A - COMPLETE PARTICIPATE RESULTS, INCLUDING FORMULAS
USED IN CALCULATIONS • — - 93
APPENDIX B - PARTICULATE FIELD DATA SHEETS — --- 108
APPENDIX C - PARTICLE SIZE FIELD DATA SHEETS 161
APPENDIX D - VISIBLE EMISSIONS FIELD DATA SHEETS — 180
APPENDIX E - EQUIPMENT CALIBRATIONS AND SMOKE READER
CERTIFICATES 229
APPENDIX F - SUPPLEMENTAL ANALYSIS 244
APPENDIX G - TRACE ELEMENT ANALYSIS 247
Scott Environmenta 1 Techroiogy Inc
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#2705-01-0380
LIST OF FIGURES
Page Number
Figure 1 - Coarse Vanadium Ore Drier • 2
Figure 2 - Coarse Vanadium Ore Storage Bins—• 3
Figure 3 - Vanadium Ore Grinder • •— 4
Figure 4 - Tailings Pond • •-•—• — 5
Figure 5 - Plan View of Hot Springs Operation, Arkansas 9
Figure 6 - Drier Cyclone Inlet North, Runs 4, 5 and 6-' 24
Figure 7 - Drier Cyclone Inlet South, Runs 4, 5 and 6 28
Figure 8 - Drier Scrubber Inlet North, Runs 4, 5 and 6 32
Figure 9 - Drier Scrubber Inlet South, Runs 4, 5 and 6 —-—• 36
Figure 10 - Dry Grinder Cyclone Inlet, Runs 1, 2 and 3 ,- 68
Figure 11 - Dry Grinder Scrubber Inlet, Runs 1, 2 and 3 72
Figure 12 - Coarse Ore Drier > 87
Figure 13 - Coarse Ore Grinder Sampling Points • • 88
Figure 14 - Particulate Sampling Train 90
Figure 15 - Patticle Size Distribution Sampling Train 91
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#2705-01-0380 -ii-
L1ST OF TABLES
Page Number^
Table 1 - Summary of Test Points and Tests Conducted • 6
Table 2 - Summary of Participate Results-Drier Cyclone Inlet North,
Runs 4, 5, 6 and 7 .---— • • 15
Table 3 - Summary of Participate Results-Drier Cyclone Inlet South,
Runs 4, 5, 6 and 7 • • •— 16
Table 4 - Summary of Particulate Results-Drier Scrubber Inlet North,
Runs 4, 5, 6 and 7 17
Table 5 - Summary of Particulate Results-Drier Scrubber Inlet South,
Runs 4, 5, 6 and 7 — 18
Table 6 - Summary of Particulate Results-Drier Scrubber Outlet,
Runs 4» 5 and 6 • ~- 19
Table 7 - Drier Control System Efficiency, Runs 4, 5 and 6 •— 20
Table 8 - Particle Size Distribution Analysis-Drier Cyclone Inlet North,
Dim 0. -~ -~ . ?1
i\U H 4-— — •««...«. —~ — — «.., — «.«.-**.«-. w .*.....*.». ~» —~_ 4_ i
Table 9 - Particle Size Distribution Analysis-Drier Cyclone Inlet North,
Pun K, _ , _ 77
f\u no —— ——. «. n» £_£„
Table 10 - Particle Size Distribution Analysis-Drier Cyclone Inlet North,
Kiln 0"""™— — ~ ™ —•«.—.«.«.-!.«.•.._M™.w- — — — —— — *_— *_ _*.*.«._..»_•.*..._«_.«,...__„—•.•••,*p.»»».-.__M.M t- ,3
Table 11 - Particle Size Distribution Analysis-Drier Cyclone Inlet South,
Table 12 - Particle Size Distribution Analysis-Drier Cyclone Inlet South,
D,m C , , , .__ 26
f\U ll*J *-\s
Table 13 - Particle Size Distribution Analysis-Drier Cyclone Inlet South,
Dim fi -- , i ?7
r\y11 u — — -...— w. »- i_t
Table 14 - Particle Size Distribution Analysis-Drier Scrubber Inlet
North, Run 4 • 29
Table 15 - Particle Size Distribution Analysis-Drier Scrubber Inlet
North, Run 5-- — - — -- 30
Table 16 - Particle Size Distribution Analysis-Drier Scrubber Inlet
North, Run 6 — • — 31
Table 17 - Particle Size Distribution Analysis-Drier Scrubber Inlet
South, Run 4 • .--__._. . 33
Table 18 - Particle Size Distribution Analysis-Drier Scrubber Inlet
South, Run 5 —- 34
Table 19 - Particle Size Distribution Analysis-Drier Scrubber Inlet
South, Run 6 • — - 35
Table 20 - Summary of Results of Opacity Readings-Drier Conveyor
Transfer Point, Run 1-— 38
Table 21 - Summary of Results of Opacity Readings-Drier Conveyor
Transfer Point, Run 2 • • 39
*
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#2705-01-0380
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LIST OF TABLES - continued
Page Number
Table 22 - Summary of Results of Opacity Readings-Drier Conveyor
Transfer Point, Run 3 • < — 40
Table 23 - Summary of Fugitive Emissions-Drier Conveyor Transfer Point,
KUH _[————«•—--••->———————---•.—..———«.—-.—,»,-.„.*,,_._—,,.-..___——»_»,».--,.»_«____._„_«._„„,_„_ ^ j^
Table 24 - Summary of Fugitive Emissions-Drier Conveyor Transfer Point,
Run 2— • • 42
Table 25 - Summary of Fugitive Emissions-Grinder Conveyor Transfer
Point, Run 1-- • • — 43
Table 26 - Summary of Results of Opacity Readings-Drier Scrubber Outlet,
i?llftl__-it.^ ,—,..,,-»».«-,.«.•.**.*..—,—i_»^*___»_-—,~, »,._ -»•» «fc «*.*.. /[ A
f\y ii j_**«" —•*- — •- — — — — — •••>«-.-—--•— — -- — -. -.--*,_» — — __-.«,«.«-.-, ^— — ^-».«. — — — _-« — — — -,_._,„_, *TLT
Table 27 - Summary of Results of Opacity Readings-Drier Scrubber Outlet,
Pi in y^ _- — _.-.-.*.*-.__, — — »- — »««--.«._.*- ___-..-__.__.._, __ /IK
r\un £_ — — •-•-"-"--'«•*'«'•-*"••-••*•*•*->" «.»,«.«._*.«.*,_.—— — -._. — —«..--_—,««,-._-*.».».*.___—»,*.___._-,. ^Q
Table 28 - Summary of Results of Opacity Readings-Drier Scrubber Outlet,
Run 3 • • 46
Table 29 - Summary of Results of Opacity Readings-Coarse Ore Bin Conveyor
Transfer Point, Run 1 • -• 47
Table 30 - Summary of Results of Opacity Readings-Coarse Ore Bin Conveyor
Transfer Point, Run 2 • • 48
Table 31 - Summary of Results of Opacity Readings-Coarse Ore Bin Conveyor
Transfer Point, Run 3- 49
Table 32 - Summary of Results of Opacity Readings-Scalping Screen, Run 1-- 50
Table 33 - Summary of Results of Opacity Readings-Scalping Screen, Run 2-- 51
Table 34 - Summary of Results of Opacity Readings-Scalping Screen, Run 3-- 52
Table 35 - Summary of Results of Opacity Readings-Baghouse Bin II Outlet,
Kun 1-————--->——-—_—_—-_-__—_—__—_——_--—_-_ i_——— ___5^
Table 36 - Summary of Results of Opacity Readings-Baghouse Bin #1 Outlet,
Run 2 ——_ .- . 54
Table 37 - Summary of Results of Opacity Readings-Baghouse Bin II Outlet,
Run 3 — - 55
Table 38 - Summary of Results of Opacity Readings-Baghouse Bin #3 Outlet,
Run 1 —• — 56
Table 39 - Summary of Results of Opacity Readings-Baghouse Bin #3 Outlet,
Run 2------ _________—_____—__________ ___ _ 5/
Table 40 - Summary of Results of Opacity Readings-Baahouse Bin 13 Outlet,
Run 3 __—— ______ 58
Table 41 - Summary of Fugitive Emissions-Coarse Ore Bin Conveyor Transfer
Points, Run 1 59
Table 42 - Summary of Fugitive Emissions-Scalping Screen, Run 1 60
Table 43 - Summary of Fugitive Emissions-Scalping Screen, Run 1 61
Scott Environment A! Technology Inc.
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12705-01-0380 -1v-
LIST OF TABLES - continued
Table 44
Table 45
Table 46
Table 47
Table 48
Table 49
Table 50
Table 51
Table 52
Table 53
Table 54
Table 55
Table 56
Table 57
Table 58
Table 59
Table 60
Table 61
Table 62
Table 63
Table 64
Paj
- Summary of Particulate Results-Grinder Cyclone Inlet,
Runs 1, 2 and 3 • •
- Summary of Participate Results-Grinder Scrubber Inlet,
Runs 1, 2 and 3 •
- Summary of Particulate Results-Grinder Scrubber Outlet,
Run 1 _--_ ~_-- -- ..__
- Particle Size Distribution Analysis-Dry Grinder Cyclone
Inlet, Run 1 • — •---
- Particle Size Distribution Analysis-Dry Grinder Cyclone
Inlet, Run 2 •
- Particle Size Distribution Analysis-Dry Grinder Cyclone
T*-tT/~i4* Diir>i ^
Illicit nil!) J-"* ~ ----- — -,_«„_„ — „_ __
- Particle Size Distribution Analysis-Dry Grinder Scrubber
Inlet, Run 1 • •--
- Particle Size Distribution Analysis-Dry Grinder Scrubber
Inlet, Run 2——— •
- Particle Size Distribution Analysis-Dry Grinder Scrubber
111 I c L 5 f\U f i ,3 """"" ***. *»»•»**.«.*,*.,- —*..,_
- Summary of Results of Opacity Readings-Grinder Conveyor
Inlet, Run 1 — — -
- Summary of Results of Opacity Readings-Grinder Conveyor
- Summary of Results of Opacity Readings-Grinder Conveyor
inlet, Run 3-— — - • — - --—-—--——-——-——-— — - — > ___ — ......
- Summary of Fugitive Emissions-Grinder Conveyor Inlet, Runs
1 7 anrl "3 --- __-
X, L CUIU ,j — — — — — — — —— — » — — ««—« — -.— —
- Summary of Results of Opacity Readings-Grinder Scrubber
Outlet, Run 1— •
- Summary of Results of Opacity Readings-Fine Ore Bin, Baghouse
f^ii'+'Ta'f'Diirtl _ _
- Summary of Results of Opacity Readings-Fine Ore Bin, Baghouse
UUti€?t^3 HUH £-•— — — — — —— ——— — «.«.«. «- * _W — K.««<..«.«.. *„-,-.*.—.*.
- Summary of Results of Opacity Readings-Fine Ore Bin, Baghouse
UU t ' Gt j HUH jf«-«- — *-*" — •- — — — — — — — — — —«. — ~« — ™ — ——— — ——*••.•• — — **-.«.•*»
- Summary of Results of Opacity Readings-Tailing Pond, Run 1
- Summary of Results of Opacity Readings-Tailing Pond, Run 2
- Summary of Results of Opacity Readings-Tailing Pond, Run 3- —
- Summary of Fugitive Emissions-Tailings Pond, Run 1
}e_Nymber_
62
63
64
65
66
67
69
70
71
73
74
75
76
77
79
80
81
82
83
£4
85
^p£&*
CSj Scott Environmenta' Technology Inc
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#2705-01-0380
1.0 INTRODUCTION
Testing to determine paniculate emissions from the processing of
vanadium ore at the Union Carbide Vanadium facility in Hot Springs, Arkansas was
conducted by Scott Environmental Technology, Inc. for the Emissions Measurement
Branch of the United States Environmental Protection Agency under Contract
No. 68-02-2813, Work Assignment No, 44. Testing was conducted from December 4
through December 8, 1979.
Particulate control systems on two process and two ore storage bin
systems were evaluated.
o Cyclone and wet scrubber on the coarse ore drier
o Baghouses on the coarse and fine ore storage bins
0 Cyclone and wet scrubber on the coarse ore grinder
Visible and fugitive emissions were also measured at various points
during the ore processing, Sampling locations used for each system are shown
in Figure 1, 2, 3 and 4. These figures also present a general description of
each process involved.
Total particulates were measured using EPA Reference Method #5 at
the inlets and outlet of the control systems (cyclones and wet scrubbers)
associated with the coarse ore drier and coarse ore grinder. Particle sizing
was measured at the inlets to the cyclones and wet scrubbers on the drier and
grinder. Opacity of the gas emitted from the scrubber outlets, baghouse
outlets, drier conveyor pickup, and scalping screen were monitored using EPA
Reference Method 19. Fugitive emissions using EPA Method #22 were measured
at five locations during the ore drying and grinding process. Table 1 presents
a summary of test points sampled and number and type of tests conducted at each
test point.
Test arrangements were made through Mr. John Powell of Union
Carbide. The following is a list of individuals present during test operations:
Individual Organization
Dennis Holzschuh EPA
Richard DeNiedo GCA, Inc.
James L. Reese Scott Environmental Technology
Frank Maccioli Scott Environmental Technology
Joseph Wilson Scott Environmental Technology
Scott Environmental Technology Inc.
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o
*-t
*-*
m
Cyclone
Inlet
Coarse Ore Conveyor
IN)
~«4
O
LH
i
O
I—"
I
o
CO
CO
o
Scrubber
Outlet "^
Manifold Duct
to Scrubber
I
ro
AAAAA AAAAA
Scrubber
Coarse Ore Conveyor to
Coarse Ore Storage Bins
FIGURE 1 - COARSE VANADIUM ORE DRIER
Union Carbide, Hot Springs, Arkansas
-------
Coarse Ore Conveyor
From Drier
Scalping Screen
aghouses.
10
c
Coarse Ore Conveyor
to Grinder
=**=
ro
~~i
o
tn
i
O
t—>
I
o
OJ
CXI
o
FIGURE 2 - COARSE VANADIUM ORE STORAGE BINS
Union Carbide, Hot Springs, Arkansas
-------
To Atmosphere
14 Scrubber Outlet
3--'Sampling Location
Conveyor From
Coarse Ore
Storage
Bins
Four
Cyclones.
Grinder Conveyor
Inlet Observation
Location
_Q
13
Scrubber Inlet
Sampling Location
^-Cyclone
Cyclone Inlet
Sampling Location
site
ro
-j
o
Ul
1
O
h~*
I
O
CO
CO
o
Fine Ore
Storaqe Bins
Rotary Ball Mill
(Grinder)
FIGURE 3 - VANADIUM ORE GRINDER -
Union Carbide,
Hot Springs, Arkansas
-------
Cyclone
Separator
FIGURE 4 - TAILINGS POND
UNION CARBIDE
HOT SPRINGS, ARKANSAS
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#2705-01-0380
-6-
TABLE 1
SUMMARY OF TEST POINTS AND TESTS CONDUCTED
Process
Drier (Figure 1)
Coarse Ore Storage Bins
(Figure 2)
Coarse Ore Grinder
(Figure 3)
Fine Ore Storage Bins
(Figure 3)
Tailings Pond
(Figure 4}
Test Point
1 - Cyclone Inlet North
2 - Cyclone Inlet South
3 - Scrubber Inlet North
4 - Scrubber Inlet South
5 - Conveyor Pickup
6 - Scrubber Outlet
7 - Conveyor Transfer
Point
8 - Scalping Screen
9 - Bin #1, Baghouse
Outlet
10 - Bin #3, Baghouse
Outlet
11 - Conveyor Inlet
12 - Cyclone Inlet
13 - Scrubber Inlet
14 - Scrubber Outlet
15 - Baghouse Outlet
16 - Tailinos Pond
5
4
4
4
4
3
Number
EPA
9
3
3
3
3
3
of Tests
Method
22
4
3
3
Sizing
3
3
3
3
3
3
3
3
1 1
3
3
3
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#2705-01-0380
-7-
lndiyj_dua_l_
Maynard Johnson
Amerino Cipoll one
Timothy Sharp
Anthony Guastella
Joseph Marino
Steve Fischer
Walter Nunes
Organization
Scott Environmental
Scott Environmental
Scott Environmental
Scott Environmental
Scott Environmental
Scott Environmental
Scott Environmental
Technology
Technology
Technology
Technology
Technology
Technology
Technology
| Scott Environmental Technology Inc.
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#2705-01-0380 -8-
2.0 PROCESS DESCRIPTION
A schematic flow diagram is shown in Figure 5. Ore with an average
grade of 1% V?0_ and 15-25% moisture is open pit mined and transported 1-2
miles by 45 metric ton (MT) (50 ton (T)) capacity trucks to a stockpile with
45,000 MT (50,000 T) capacity. Small quantities of South African slag
(5-25% V90~) are also processed. Ore passes through one of two grizzlies with
w >3
12 inch openings into an underground conveyor to the primary crusher. The
crusher is an impact hammer type which normally operates at 73-109 MT (80-120T)
per hour and reduces ore to two inches. The crushed ore is then dried using
natural gas as fuel at 100°C. Ore is then transported to one of five coarse
ore bins with a total capacity of 3400 MT (5,000 T). Just prior to entering
the bin, a screen removes ore >2 inches from the ore. Dry grinding uses a
Hardinge semi-autogenous (201 x 6') with a capacity of 68 MT (75 T)/hour.
Material is air conveyed to a gyrator that returns coarse material (>100 mesh)
for regrinding. A dry cyclone separates product from air stream and conveys
it to the fine ore bin with 2300 MT (2,500 T) capacity. Ore goes to the
extruder building where water is added to blenders and pug mills to result
in 12-14% moisture content. Salt required for roasting is added at this point.
Ore is extruded at approximately 1 inch diameter core for permeability. The
roasting circuit includes a preheater, kiln and cooler. Product is dried to
10% moisture and is then fed through a wet AMV (ammonium meta vanadate) circuit
to the MVO "dryer-reactor". The final product, a dry black powder, is sent to
a surge bin, packaged in cylinders and transported by rail cars.
Tailings are produced at a rate of 1,400 MT (1,500 T)/day by operations
and are pumped as a slurry 1,000 to 6,000 feet. The slurry receives no treatment
after leaving the thickener circuit.
A description of the control equipment that was tested is given in
the following sections.
A, Coarse Ore Dryer
A Joy Model "T" Turbulaire wet scrubber preceded by a dry cyclone
controls emissions from conveyor transfer points to the dryer. Design outlet
parameters are a flow rate of 61.4m3/sec. (130,000 cfm) at 175°C (350°F) and
design outlet parameters of 52m3/sec. (110,000 cfm ) at 81°C (180°F). Inlet
moisture is approximately 401 and water is applied at a rate of 85 gpm. Operating
pressure drop is 10 inches W.G.
Scott Envinonmenta! Technology Inc.
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PfS-ORY
MATERIAL.
AND FLAXiNG
COARSE
ons OIKS
EXTRUDING
V- o
SALT
MVO
=*=
I
o
I — I
I
o
OJ
CO
o
.PACKAGING
FIGURE 5 - PLAN VIEW OF HOT SPRINGS OPERATIONS, ARKANSAS
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12705-01-0380 -10-
B. Dry Grinder
A Joy Model "T" Turbulaire wet scrubber preceded by a cyclone controls
emissions from the grinder with an operating pressure drop of 10 inches wet
3
gauge. Design inlet parameters are a flow rate of 8.5m /sec. (18,000 cfm) at
59°C (140°F) and design outlet parameters are 7.1m /sec. (15,000 cfm) at
32°C (90°F). Liquid is applied at 20 gpm rate.
2.1 PROCESS SAMPLES
Ore samples were taken to ascertain whether a correlation between ore
moisture content and inlet emissions could be developed. On December 5, 1979,
two samples were taken from the conveyor feeding the dry grinding operation.
On December 8, 1979, two ore samples were taken from the conveyor belt between
the primary crusher and coarse ore dryer. The results are noted on Page 245.
2.2 PROCESS OPERATION - COARSE ORE DRYER
The drier continuously receives ore from the primary crusher except
for shift changes, every 8 hours, or when the coarse ore bins are filled. Process
data for the 3 weeks prior to emission testing on December 6-8, 1979 shows an
hourly process rate of 83 MT (93 T). Reduced process rates are primarily due
to a high moisture ore (>15%) from the East Wilson Pit. The dryer process rates
are given below in metric tons/hour.
Time Dec. 6 Dec. 7 Dec. 8
0
52
0 68
99* 89*
76* 88*
82* 91*
76*
81
*0re from North Wilson Pit.
8:30 AM
9:30 AM
10:30 AM
11:30 AM
12:30 PM
1:30 PM
2:30 PM
3:30 PM
4:30 PM
5:30 PM
6:30 PM
7:30 PM
8:30 PM
9:30 PM
10:30 PM
y*t r r 11:30 PM
iX) Scott Environmental Technology Ire.
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52
79
78
77 "
79
82
93
72*
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#2705-01-0380
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Another parameter checked was the dryer firebox temperature which
maintained its normal operating temperature (1000°C). The pressure drop of the
scrubber was also measured. Normal operating range is 9-10.5 inches of water.
During the December 8 test, the readings were:
Time Ap, (jnches^_ waterji_
8:30 a.m.
9:00 a.m.
9:30 a.m.
10:00 a.m.
10:30 a.m.
11:00 a.m.
11:30 a.m.
12:00 p.m.
12:30 P.m.
1:00 P-rn.
1:30 P.ro.
2:00 P-w.
2:30 p.m.
3:00 P.m.
3:30 p. in.
4:00 p.m.
A summary of Methods 9 and 22 observations
Method 9
Location Date
Scrubber Outlet 12-6-79
12-7-79
12-8-79
Conveyor Transfer Point 12-8-79
Method
I nraf ion Date
L,v/Vv4 v i Uli „
Convevor Transfer Point 12-7-79
14
14
13
11.5
12.5
12
11.5
12
12
11.5
12
12
12.5
12
12
12.5
follows:
No. of 6-min.
intervals
10
17
18
30 '
22
Test Duration
(Seconds) __
5700
Opacity Reading (%}
(6-min.average)
Average Maximum
1
1
0
0
5
5
0
0
Fugitive Emissions
Seconds %
0
0
Scott Environmental Technology Inc
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#2705-01-0380
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2.3 PROCESS OPERATION - DRY GRINDING
The grinder continuously receives ore from the coarse ore bins except
for shift changes. Process data for the 3 weeks prior to testing showed an hourly
process rate of 59 MT (65 T). Inspection of weight-belt scales and meters showed
no gross abnormalities. The hourly processing rates are given below in
metric tons/hour.
Time
Dec. 4
Dec, 5
8:30 a.m.
9:30 a.m.
10;30 a.m.
11:30 a.m.
12:30 p.m.
1:30 p.m.
2:30 p.m.
3:30 p.m.
4:30 p.m.
5:30 p.m.
6:30 p.m.
7:30 p.m.
0
59
58
58
63
53
41
45
0
61
66
64
62
62
64
59
A summary of Methods 9 and 22 observations follows:
Method 9
No. of 6-min.
Opacity Reading (1
(6-min. average)
Location
.veyo
11
i)
•ubbe
r Inlet
it
11
r Outlet
Date
12-4-79
12-5-79
12-5-79
12-5-79
intervals
21
7
10
10
Average
0
0
0
25
Maximu
0
0
0
25
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#2705-01-0380
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Method 22
Test Duration
Fugitive Emission:
Location
Conveyor Inlet.
it H
11 it
Date,
12-4-79
12-5-79
12-5-79
(seconds)
6055
4500
4380
Seconds
0
0
0
o/
0
0
0
2.4 PROCESS OPERATION-COARSE ORE STORAGE BINS
A summary
Location
Conveyor Transfer
Conveyor Transfer
Scalping Screen
Scalping Screen
Baghouse Bin #1 (
Baghouse Bin fl (
Baghouse Bin 13 (
Location
Conveyor Transfer
Scalping Screen
Scalping Screen
of Methods #9 and #22 follow:
Date
Point 12/5/79
Point 12/8/79
12/5/79
12/8/79
outlet) 12/8/79
outlet) 12/9/79
outlet) 12/5/79
Date
Point 12/8/79
12/5/79
12/8/79
Method 9
No. of 6-min.
Intervals
10
20
10
20
26
10
23
Method 22
Test Duration
(Seconds)
7200
3600
7200
Opacity Reading (%)
{6-min. average)
Average Maximum
U 0
2 4
15 24
31 45
5 9
6 8
3 7
Fugitive Emissions
Seconds %
2548 35
3600 100
7200 100
Oj Scott Environmental Technotagy Inc.
-------
12705-01-0380 -14-
3,0 SUMMARY AND DISCUSSION OF RESULTS
3.1 COARSE ORE DRIER
Testing for particulates was conducted at the inlet to two cyclone
scrubbers, two wet scrubbers, and the wet scrubber outlet. Particle sizing
was measured at the inlets of the cyclones and wet scrubbers. Visible
emissions were monitored at the conveyor pickup and outlet using EPA Method
19 and fugitive emissions were monitored using EPA Method #22 at the conveyor
pickup. Results of particulate testing are summarized in Tables 2 through 6.
The control system efficiency of the coarse ore drier is summarized in Table 7.
Complete particulate results, including formulas used in the calculations,
are included in Appendix A. Field data sheets are included in Appendix B.
The particulate sampling at the cyclone inlets and scrubber inlets
was complicated by the high moisture and particulate concentration at these
locations. The heavy particulate loading, combined with the moisture caused
the particulate to agglomerate and quickly plug the filter. Because of the
lack of uniform duct dimensions up and downstream from the inlet sampling
locations, sampling was initially attempted at 48 points. However, numerous
filter changes were necessary. For the later test runs, the number of sample
points was reduced in order to reduce the sampling time. Glass wool was also
inserted into the filter holder to collect some of the particulate and to keep
the filter from plugging. At several inlet locations it was not possible to
sample in the bottom port due to a buildup of particulate in the duct.
During the testing, several different types of ores with varying
moisture content were processed in the drier. These different ores caused the
stack gas temperature and moisture content to vary at the sampling locations
which made isokinetic sampling difficult. The first test run was not isokinetic
at two of the test locations due to an underestimate of the stack moisture
content. The isokinetic rates of the later test runs were affected by the
varying stack gas temperature. Four test runs were made at the inlets in an
effort to obtain valid results. Only one test run was made on December 7, 1979
due to a shutdown of the drier. The coarse ore bins were filled to capacity
necessitating the shutdown.
Results of the particle size analysis at the cyclone inlets and
scrubber inlets are summarized in Tables 8 through 19 and in Figures 6 through
9. Field data sheets are included in Appendix C.
Scott Environmental Technology Inc.
-------
12705-01-0380
-15-
TABLE 2
SUMMARY OF PARTICIPATE RESULTS
Drier North Cyclone Inlet
Date:
Time Started:
Time Ended:
Run No:
Gas Flow Rates, (dscfm):
Actual Gas Flow Rate
(acfm):
Participate Concentration
(gr/dscf):
Parti cul ate Mass Flow
Rate (Ibs/hr):
12-6
1924
2330
4
12,680
22,780
52.01
6520
12-7
1150
1320
5
14,470
25,270
87.23
8450
12-8
0925
1030
6
12,090
26,580
99.64
9580
12-8
1445
1600
7
14,690
27,980
71.54
8390
jfy); Scott Environmental Technology Inc
-------
#2705-01-0380
-16-
TABLE 3
SUMMARY OF PARTICULATE RESULTS
Drier Cyclone Inlet South
Date;
Time Started:
Time Ended:
Run No:
Gas Flow Rates, (dscfra):
Actual Gas Flow Rate
(acfm):
Participate Concentration
(gr/dscf):
Parti cul ate Mass Flow
Rate (Ibs/hr):
12-6
1839
1943
4
12,680
22,780
38.76
4210
12-7
1305
1709
5
14,470
25,270
83.45
10,350
12-8
0930
1035
6
12,090
26,580
37.62
3900
12-8
1400
1540
7
14,690
27,980
62.39
7860
j{Y)j Scott Environment! [Technology Ire
-------
#2705-01-0380
-17-
TABLE 4
SUMMARY OF PARTICULATE RESULTS
Drier Scrubber Inlet North
Date:
Time Started:
Time Ended:
Run No:
Gas Flow Rates, (dscfm):
Actual Gas Flow Rate
(acfm):
Particulate Concentration
(gr/dscf):
Particulate Mass Flow
Rate (Ibs/hr):
12-6
1913
2330
4
15,090
29,560
8.022
1040
12-7
1200
1330
5
14,170
24,060
5.785
703
12-8
0930
1035
6
14,660
25,440
6.486
815
12-8
1448
1628
7
14,470
25,510
10.801
1340
Scott Environmental Technology Inc.
-------
12705-01-0380
-18-
TABLE 5
SUMMARY OF PARTICULATE RESULTS
Drier Scrubber Inlet South
Date:
Time Started;
Time Ended:
Run No:
Gas Flow Rates, (dscfm):
Actual Gas Flow Rate
(acfm):
Participate Concentration
(gr/dscf):
Particulate Mass Flow
Rate (Ibs/hr):
12-6
0930
1035
4
14,320
26,730
10.99
1350
12-7
1030
1305
5
15,330
27,760
9.28
1220
12-8
0900
1100
6
19,730
36,010
5.98
1010
12-8
1400
1540
7
15,300
30,810
20.69
2710
Scott Environmental Technobgy Inc
-------
#2705-01-0380
-19-
TABLE 6
SUMMARY OF PART1CULATE RESULTS
Drier Scrubber Outlet
Date:
Time Started:
Time Ended:
Run No:
Gas Flow Rates, (dscfm):
Actual Gas Flow Rate
(acfm):
Parti cul ate Concentration
(gr/dscf):
Particulate Mass Flow
Rate (lbs/hr):
12-6
1817
2005
4
40,800
64,240
0.0526
18.4
12-7
1019
1206
5
34,650
55,130
0.0187
5.6
12-8
0828
1029
6
40,680
61,630
0.0442
15.4
i fs)' Scott Environmental Technobqv Inc
-------
12705-01-0380 -20-
TABLE 7
DRIER CONTROL SYSTEM EFFICIENCY
Date: 12/6/79 12/7/79 12/8/79
Run No.: 456
Total Particulate Flow Rate
at Cyclone Inlet, Ibs/hr 10,730 18,800 14,860*
Total Particulate Flow Rate
at Scrubber Inlets, Ibs/hr 2,390 1,923 2,940*
Total Particulate Flow Rate
at Scrubber Outlet, Ibs/hr 18.4 5.6 15.4
Efficiency of Cyclones, % 77,7 89.8 80.2
Efficiency of Scrubber, % 99.2 99.7 99.5
Efficiency of Overall System, % 99.8 99.97 99.90
* Average of Runs 6 & 7.
Irv
-------
#2705-01-0380
-21-
TABLE 8
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-6-79
Time: 2330
Sampling Location
Traverse Point No, Sampled: 21
Run No.: 4
Pbar(in. Hg): 29.48
Drier Cyclone Inlet stack Tei?P- {°F): 297-°
North Sample Time (Min): .67
Sample Volume (cf): .491
Moisture (% H~0): 27.6
Meter Temperature (°F): 48.0
Flow Setting, iH (in. H?0): 2.25
Nozzle Diameter (In.): ""c
.375
Sample Flow Rate {at stack conditions) - 1.03 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(ing)
475. 452
156.10
110.90
28.55
13.15
1.85
.50
.25
.50
%
60.39
19.82
14.08
3.62
1.67
.23
.06
.03
.06
Cumulative
*
100.00
39.60
19.77
5.69
2.06
.39
.15
.09
.06
ECD1
(Hjcrometers )
10.85 and larger
6.92
4.55
- 3.14
2.01
1.02
.61
.41
£-41
Total 787.25
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technology Inc.
-------
#2705-01-0380
-22-
TABLE 9
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-6-79 Ph^1""- H9):
Time: 2332 fj ti
Sampling Location: Drier Cyclone Inlet NortnX^^1™:;
Traverse Point No. Sampled: 21
Run No.: 5
29.48
Moisture (% H-O): Q27,6
Meter Temperature ( F): 47.0
Flow Setting, AH (in. O): 2.25
Nozzle Diameter (In.): .375
Sample Flow Rate (at stack conditions) - 1.10 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
386. 452
219.65
203.90
59.80
20.60
6.20
1.40
3.00
5.50
42.63
24.23
22.49
6.59
2.27
.68
.15
.33
.60
Cumulative
%
100.00
57.36
33.13
10.64
4.04
1.77
1.09
.93
ECDA
(Micrometers)
10.48 and larger
6.69
4.40
3.04
1.94
.99
.59
.39
.60
<.39
Total 906.50
1
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technology Inc.
-------
#2705-01-0380
-23-
TABLE 10
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-6-79
Time: 2334
Pbar(in. Hg): 29.43
lime: ^JJt e, , T /or\
Sampling Location: Drier Cyclone Inlet Northftac.k r^P. F):
9
Point No. Sampled: 21
Run No.: 6
i«7
Moisture (% O): 27.6
Meter Temperature ( F): 48.0
Flow Setting, AH (in, H?0): 2-25
Nozzle Diameter (In.): l -375
Sample Flow Rate (at stack conditions) - 1.31 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
249.35*
180,00
130.95
69.70
35.00
8.00
.55
1.00
2.50
36.82
26.58
19.34
10.29
5.16
1.18
.08
.14
.36
Cumulative
%
100.00
63.17
36.58
17.24
6.94
1.77
.59
.51
ECD1
(Micrometer
9.57 and
6.13
4.02 '
2.78
1.78
.90
.54
.35
•s)
larger
,
.36
<.35
Total 677.05
ECD - Effective Cutoff Diameter of preceding plate.
o
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technology Inc.
-------
; flit, t _-. ,. H CO
2
Hhfi.
99.09
99.5 59.8
99
0.01
HI
" *" •"• <••} *"-t~V
S-Lffll
FIGURE 6
DRIER CYCLONE INLET-NORTH
RUN 5 •
RUN 6
—-A .
Cumulative %, Less Than Stated
Particle Size
-------
12705-01-0380 ~25~
TABLE 11
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-6-79 PkaJin. Hg): 29.48
T* O"3Q£ Do. i
Sampl'ing Location;Dner Cyclone Inlet South$tac.k Temp. { F): 284.0
Traverse Point No. Sampled: 20 ^amp e Time (Mm): -262
R M . . K Sample Volume (cf): .130
Run N°" 4 Moisture (% H?0): 20.3
Meter Temperature ( F): 40.0
Flow Setting, m {in. H?0): 1.82
Nozzle Diameter (In.): .375
Sample Flow Rate (at stack conditions) - .64 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(wig)
259. 102
6.20
2.00
,70
.40
.40
.00
.00
.20
%
96.31
2.30
.74
.26
.14
,14
.00
.00
.07
Cumulative
%
100.00
3.68
1.37
.63
.37
.22
.07
.07
.07
ECD1
(Hicrometers)
13.73 and larger
8,68
5.74
3.97
2.53
1.30
.78
.53
4.53
Total 269.00
ECD - Effective Cutoff Diameter of preceding plate.
p
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
! Scott Environmental Technology Inc.
-------
12705-01-0380
-26-
TABLE 12
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-6-79 Pbar^1n* Hg^: 29'48
Location: Drier Cyclone Inlet Souttgack Temp (°F): 284^0
Sailed: 20 gj ; JJ^ } s '?&
Moisture (*O): 27.7
Meter Temperature { F): 40.0
Flow Setting, M (in. H20): 1-82
Nozzle Diameter (In.): >375
Sampling
TraJerse9 Point No
Run No': 5
Sample Flow Rate (at stack conditions) - .85 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(ing)
163. 30Z
2.30
.75
.40
.30
.50
.40
.15
.20
97.02
1.36
.44
.23
.17
.29
.23
.08
.11
Cumulative
%
100.00
2.97
1.60
1.15
.92
.74
.44
.20
ECD1
(Microineters )
11.91 and
7.57
4.99
3.45
2.20
1.12
.68
.45
larger
.11
<.45
Total 168.30
1
ECD - Effective Cuto'ff Diameter of preceding plate.
y
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technoky^y Inc.
-------
#2705-01-0380
-27-
TABLE 13
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date:
12-6-79
Pbar^*n"
30'17
Traverse Point No. Sampled:
nM~.
Run No':
20
Location: Drier Cyclone Inlet Soutf|tac.k T^P- j^}: 399.0
Samp e Time (Mm): -253
Sample Volume (cf): -119
Moisture (*H?0): 26.5
Meter Temperature ( F) : 41
Flow Setting, AH (in. H?0)
Nozzle Diameter (In.):
1-82
375
Sample Flow Rate (at stack conditions) - .65 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(rug)
221.002
.80
.45
.30
.15
.20
.35
.20
.20
98.81
.35
.20
.13
.06
.08
.15
.08
.08
Cumulative
100.00
1.18
.82
.62
.49
.42
.33
.17
.08
ECD1
(Hlcrometers)
14.44 and larger
9.14
6.04'
4.18
2.67
1.37
.83
.56
<.56
Total 223.65
1
ECD - Effective Cutoff Diameter of preceding Dlate.
-------
99,99
90,5 59.0
09 98
1 0.5 O.Z O.I 0.05
0.01
h/ sm
FIGURE 7
DRIER CYCLONE INLET-SOUTH
RUN 4
RUN 5
RUN 6
Cumulative %, Less Than Stated
Particle Size
-------
#2705-01-0380 -29-
TABLE 14
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-8-79 pba/in' Hg': 3°"17
Sampling Location: Drier Scrubber Inlet No|tack Temp. (°F): 321.0
Traverse Point No. Sailed: 22 (6) |«p J ^Mln,. ;50g
Run NO': 4 Moisture (% H?0): 25.2
Meter Temperature ( F): 58,0
Flow Setting, M (in. H?0): 2-35
Nozzle Diameter (In.): -375
Sample Flow Rate (at stack conditions) - 1.18 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(rag)
210. 602
40.50
28.90
16.35
9.30
2.75
.20
.40
.30
%
68.08
13.09
9.34
5.28
3.00
.88
.06
.12
.09
Cumulative
*
100.00
31.91
18.81
9.47
4.18
1.18
.29
.22
.09
ECD1
(Micrometers)
10,25 and larger
6.55
4.30
2.97
1.90
.96
.58
.38
4.38
Total 309.30
ECD - Effective Cutoff Diameter of preceding plate.
p
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
I Scott Environmental Technology Inc.
-------
12705-01-0380 ~30'
TABLE 15
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-8-79 pbar^1n' Hg^: 30'14
SSl1ng23L«at1on: Drier Scrubber Inlet No. ^Tej. f°F) : 399^0
Traverse Point No. Sailed: 22 gjlj £«M»n) _.417
Run No': Moisture (% H?0) : 25.2
Meter, Temperature ( F) : 58.0
Flow Setting, M (in. H?0) : 2.35
Nozzle Diameter (In.): .375
Sample Flow Rate {at stack conditions) - 1.35 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 206.602 61.06 100.00 9.96 and larger
2 65.10 19.24 38.93 6.39
3 32.90 9.72 19.69 4.18'
4 18.05 5.33 9.97 2.89
5 10.95 3.23 4.64 1.85
6 3.50 1.03 1.40 .93
7 .15 .04 .36 .56
8 .35 .10 .32 .37
Back-up
Filter -75 -22 -22 *-37
Total 338.35
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
ScotrEnvironmentanecficofogylnc
-------
12705-01-0380 -31-
TABLE 16
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-8-79 pbar^1n< Hg^: 30'14
Sampling Location: Drier Scrubber Inlet No, Stack Temp. (°F): 399,0
Traverse Point No. Sampled: 22 Samp e Time (Mm): .50
p,tn Wn . 6 Sample Volume (cf : -436
Run N°" Moisture (% HO): 25,2
Meter Temperature ( F): 58.0
Flow Setting, AH (in. H?0): 2.35
Nozzle Diameter (In.): -375
Sample Flow Rate (at stack conditions) - 1-23 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 196.25 60.58 100.00 10.43 and larger
2 47.30 14.60 39.41 6,68
3 31.30 9.66 24.81 4.38'
4 25.75 7.94 15.15 3.03
5 15.40 4.75 7.20 1-94
6 6.95 2.14 2.45 -98
7 .50 .15 .30 -59
8 .20 .06 .15 -39
• .30 .09 .09
Total 323.95
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
I vSJ Scott Environment*- .1 Technology Inc.
-------
0,01
"rH^i'lIrn
FIGURE 8
DRIER SCRUBBER INLET-NORTH
RUN 4
RUN 5
A.L_f
t-!:-
RUN 6
Cumulative %, Less Than Stated
Particle Size
-------
#2705-01-0380 -33-
TABLE 17
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-7-79 P (in. Hg): 29.66
Time- 2330 bar 0
Sampling Location: Drier Scrubber Inlet So.Stad< Temp. F): 216 0
Traverse Point No. Sampled: 22 Samp e Time (Mm): .583
Rljn Nn . 4 Sample Volume (cf): .587
KUn N°" Moisture (% H?0): 28.5
Meter Temperature { F): 57.0
Flow Setting, AH (in. H?0): 3.2
Nozzle Diameter (In.): -375
Sample Flow Rate (at stack conditions) - 1.38 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
234. 00Z
64.90
38.60
14.20
6.00
1.50
.50
,40
.80
%
64.83
17.98
10.69
3.93
1.66
.41
.13
.11
.22
Cumulative
100.00
35.16
17.17
6.48
2.54
.88
.47
.33
.22
ECD1
(Micrometers )
8.93 and larger
5.73
3.75
2.59
1.66
.84
.50
.33
<.33
Total 360.90
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
(\) Scott Environmental Technology Inc.
-------
#2705-01-0380 -34-
TABLE 13
PARTICLE SIZE DISTRIBUTION ANALYSIS
P, (in. Hg): 29.66
Drier Scrubber Inlet So. Stack Temp. (°F): 215.0
Run N°': 5 Moisture (2 HO): 28.5
Meter Temperature ( F): 57.0
Flow Setting, AH (in. H?0): 3,2
Nozzle Diameter (In.): -375
Sample Flow Rate (at stack conditions) - 1.23 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) % % (Micrometers)
1 254.55Z 76.92 100.00 9.47 and larger
2 38.30 11.57 23.07 6.06
3 24.00 7.25 11.49 3.98"
4 9.20 2.78 4.24 2.75
5 3.70 1.11 1.46 1.76
6 .60 .18 -34 .89
7 ,20 .06 -16 .53
3 .00 .00 .10 .35
Back-up ,n -„ * oc
Fllte/ .35 .10 .10 <.35
Total 330.90
1
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmenta1 Technology Inc.
-------
^2705-01-0380 oc
-oo-
TABLE 19
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-7-79 p (in. Hg): 29.66
Time: 2334 J: . T (o <
Sampling Location: Drier Scrubber Inlet So.Jtac* T^P- J): 215.0
Traverse Point No. Sampled: 22 $
-------
99.M
I 0,5 0,2 0,1 0,05 O.OT
70 60 50 40 30 20
t; tijji iM i
FIGURE 9
DRIER SCRUBBER INLET-SOUTH
RUN 4
RUN 5
RUN 6
t •—-..——-I •—t—-4 —*
_ -.jrrl I-il
Particle Size
Q
A .}-T=
TTir
1 J 1 J I i | I j-i-[ -i-n 1 1 | i i |
ill! i i 1 i I I 1 1 111 ! , i ! 1
nan Stated
se
im IN minim i i
' * i
-
_
!
-*—
"*- --"
••r~r~
f t *
< '
.1-1
i!
i
i j
t * *
1
t
' t
j i
h
i
i
,l
1
-
~ j —
_
~
• •[ "
T
-
t — .
1
*""
*
„„..
i t
!
• 1
!i.l
|j!
;i
t!
io_
'i
I ' ••
t
...
}
- ••
-"
c.o:
-------
12705-01-0380 -37-
The results of visible emissions observations at the drier conveyor
belt transfer point are summarized in Tables 20 through 22 (smoke density)
and Tables 23 through 25 (fugitive emissions). Opacity readings at the
scrubber outlet are summarized in Tables 26 through 28.
3.2 COARSE ORE STORAGE BINS
Visible emissions were monitored at the coarse ore bin conveyor
transfer point, the scalping screen, and baghouse #1 outlet and baghouse #3
outlet using EPA Method #9. Fugitive emissions v/ere monitored at the coarse
ore bin transfer point and at the scalping screen using EPA Method #22.
Method #9 results are summarized in Tables 29 through 40 and Method #22 results
are summarized in Tables 41 through 43.
3.3 COARSE ORE GRINDER
Testing for participate matter at the coarse ore grinder was conducted
at the cyclone inlet, the scrubber inlet and the scrubber outlet. Visible
emissions v/ere monitored at the conveyor transfer point at the grinder with EPA
Methods #9 and #22 and at the scrubber outlet with EPA Method #9. Due to the
high opacity at the scrubber outlet, it was not felt that the scrubber was oper-
ating efficiently. One test only was run at this location to determine the
magnitude of the emissions.
Results of the particulate testing are summarized in Tables 44 through
46. Complete particulate results, including formulas used in the calculations
are included in Appendix A. Field data sheets are included in Appendix B.
Results of Test Run 13 at the scrubber inlet are not considered
representative because a leak was discovered in a crack in the filter holder at
the end of the test run. It is not known exactly when the crack developed. The
first test run at the cyclone inlet was under isokinetic. There is no apparent
reason for the low sampling rate except possibly an error in setting, the
nomograph.
Results of the particle size analysis at the cyclone inlet and the
scrubber inlet are shown in Tables 47 through 52, and Figures 9 and 10. Field
data sheets are included in Appendix C.
Results of the visible emissions observations at the conveyor inlet
are summarized in Tables 53 through 55 (Method #9) and Table 56 (Method #22).
Visible emissions observations at the scrubber outlet are summarized in
Table 57.
Scott Environmental Technology Inc
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12705-01-0380
-38-
TABLE 20
SUMMARY OF RESULTS OF OPACITY READINGS
Location: §Her Conveyor Transfer Point
Test Run No.: 1
Date: 12-8-79
Color of Plume: White
Stack Height: 4'
Distance to Stack: 15'
Wind Direction:East 0-5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End Sum
1300 1306 0
1306 1312 0
1312 1318 0
1318 1324 0
1324 1330 0
1330 1336 0
1336 1342 0
1342 1348 0
1348 1354 0
1354 1400 0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
11
12
OVERALL AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Scott Environmental Technokxjy Inc.
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#2705-01-0380
-39-
TABLE 21
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Drier Conveyor Transfer Point
Test Run No.: 2
Date: 12-8-79
Color of Plume: White
Stack Height: 4'
Distance to Stack: 20'
Wind Direction: E 5-10 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time . Opacity
Start End Sum Average
1200 1206 0 0
1206 1212 0 0
1212 1218 0 0
1218 1224 0 0
1224 1230 0 0
1230 1236 0 0
1236 1242 0 0
1242 1248 0 0
1248 1254 0 0
1254 1300 0 0
11
12
OVERALL AVERAGE 0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
' Scott Environmental Tethndcxiy Inc
-------
12705-01-0380
-40-
TABLE 22
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Drier Conveyor Transfer Point
Test Run No.: 3
Date: 12-8-79
Color of Plume: White
Stack Height: 3'
Distance to Stack: 15'
Wind Direction: E 5 niph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time Opacity
Start End Sum Average
1400 1406 0 0
1406 1412 0 0
1412 1418 0 0
1418 1424 0 0
1424 1430 0 0
1430 1436 0 0
1436 1442 0 0
1442 1448 U 0
1448 1454 0 0
1454 1500 0 0
11
12
OVERALL AVERAGE 0
13
14
15
16
17
18
19
i,
20
Set Time Opacity
Number Start End Sum Average
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
>! Scon Environments I Technology Inc
-------
#2705-01-0380 -41-
TABLE 23
SUMMARY OF FUGITIVE EMISSIONS
Date: • 12-6-79
Location: Drier Conveyor Transfer Point
Run No.: 1
Time Started: 0436
Time Ended: 0515
Test Duration (seconds): 1800
Cumulative Duration of
Emissions (seconds): 6^7
Percentage of Test Duration with
Emissions (%): 37>1%
Average (Percent): 37.1%
Scott Environmental Technofoqv IDC.
-------
12705-01-0380 -42-
TABLE 24
SUMMARY OF FUGITIVE EMISSIONS
Date: 12/7/79
Location: Drier Conveyor Transfer Point
Run No.: 2
Time Started: 1100
Time Ended: 1317
Test Duration (seconds): 5700
Cumulative Duration of
Emissions (seconds): 0
Percentage of Test Duration with
Emissions (%): 0
Average (Percent): 0
Scott Environmental Technofosy Inc.
-------
#2705-01-0380
-43-
TABLE 25
SUMMARY OF FUGITIVE EMISSIONS
Date: 12/8/79
Location: Grinder Conveyor Transfer Point
Run No,: ' 1
Time Started: 0921
Time Ended: 1115
Test Duration (seconds): 4530
Cumulative Duration of
Emissions (seconds): 50
Percentage of Test Duration with
Emissions (%}: 1«1^
Average (Percent): \.\%
!tV) Scott Environment;.! Technokxzv inc.
-------
#2705-01-0380
-44-
TABLE 26
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Dryer Scrubber Outlet
Test Run No.: 1
Date: 12-6-79
Color of Plume: White
Stack Height: 150'
Distance to Stack:250'
Wind Direction: West 0-5 rnph
Sky Description:Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End Sum
1610 1616 0
1616 1622 10
1622 1628 0
1628 1634 0
1634 1640 0
1640 1646 20
1646 1652 90
1652 1658 95
1658 1704 55
1704 1710 5
Opacity
Average
0
0
0
0
0
0
5
5
0
0
11
12
OVERALL AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
i(\): Scott Environmental Technology Inc
-------
#2705-01-0380
-45-
TABLE 27
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Dryer Scrubber Outlet
Test Run No.: 2
Date: 12-7-79
Color of Plume: White
Stack Height: 150'
Distance to Stack: 250'
Wind Direction: West 0-5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
•16
17
Time
Start End
1020
1026
1032
1038
1044
1050
1056
1102
1108
1114
1120
1126
1132
1138
1144
1150
1156
1026
1032
1038
1044
1050
1056
1102
1108
1114
1120
1126
1132
1138
1144
1150
1156
1202
Sum
0
0
0
0
0
0
0
0
0
0
0
0
90
85
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
5
5
0
0
0
18
19
OVERALL
AVERAGE
0
20
Set Time Opacity
Number Start End Sum Averaae
.21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
. 3 \, \ i C<-/-vt-* C*-*» »irj«"*.r'
-------
#2705-01-0380
-46-
TABLE 28
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Dryer Scrubber Outlet
Test Run No.: 3
Date: 12-8-79
Color of Plume: White
Stack Height: 150'
Distance to Stack: 300'
Wind Direction: N 5-10 rnph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
Time
Start End
0829
0835
0841
0847
0853
0859
0905
0911
0917
0923
0929
0935
0941
0947
0953
0959
1005
1011
0835
0841
0847
0853
0859
0905
0911
0917
0923
0929
0935
0941
0947
0953
0959
1005
1011
1017
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
19
20
OVERALL AVERAGE
0
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38 . . .
39
40
;i Scott Environment! Technology Inc
-------
12705-01-0380
-47-
TABLE 29
SUMMARY OF RESULTS OF OPACITY READINGS
Coarse Ore Bin
Location: Conveyor Transfer Point
Test Run No.: i
Date: 12-5-79
Color of Plume: White
Stack Height:
Distance to Stack:lo1
Wind Direction: SW 5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
0940. 0946
0946 0952
0952 0958
0958 1004
1004 1010
1015 1021
1021 1027
1027 1033
1033 1039
1039 1045
Sum
0..
0
0
0
0
0
0
0
0
0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
11
12
OVERALL AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Fnrvirnnnrv*n
Inr
-------
12705-01-0380
-48-
TABLE 30
SUMMARY OF RESULTS OF OPACITY READINGS
Coarse Ore Bin
Location: Conveyor Transfer Point
Test Run No.: 2
Date: 12-8-79
Color of Plume: White
Stack Height: NA
Distance to Stack: NA
Vfind Direction: West 5-10 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End Sum
1147 1153 30
1153 1159 60
1159 1205 5
1205 1211 ' 5
1211 1217 '35
1227 1233 30
1233 1239 45
1239 1245 65
1245 1251 55
1251 1257 25
Opaci ty
Average
0
0
0
0
0
0
0
5
0
0
11
12
OVERALL AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
I CD '
Environments ! T^chnofc^y Inc
-------
12705-01-0380
_49-
TABLE 31
SUMMARY OF RESULTS OF OPACITY READINGS
Coarse Ore Bin
Location: Conveyor Transfer Point
Test Run No,: 3
Date: 12-8-79
Color of Plume: White
Stack Height: NA
Distance to Stack: NA
Wind Direction: West 5-10 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
1306
1312
1318
1324
1330
1406
1412
1418
1424
1430
1312
1318
1324
1330
1336
1412
1418
1424
1430
1436
Sum
30
30
45
40
45
40
95
Opacity
Average
0
0
0
0
0
0
5
100 5
70
75
5
5
11
12
OVERALL
AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sura Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
*^-J"V»»' HT »
-------
12705-01-0380
-50-
TABLE 32
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Scalping Screen
Test Run No.: 1
Date: 12-5-79
Color of Plume:White
Stack Height: NA
Distance to Screen 10'
Wind Direction: SW 5-10 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
1050 1056
1056 1102
1102 1108
1108 1114
1114 1120
1135 1141
1141 1147
1147 1153
1153 1159
1159 1205
Opacity
Sum Average
555 25
320 15
285 10
270 10
390 15
405 15
185 10
230 10
455 20
575 25
11
12
OVERALL AVERAGE
15
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
I Scott Environmental Technology Inc.
-------
#2705-01-0380
-51-
TABLE 33
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Scalping Screen
Test Run No.: 2
Date: 12-8-79
Color of Plume: White
Stack Height: NA
Distance to Screen: 10'
Wind Direction: SW 5-10 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
1454 1500
1500 1506
1506 1512
1512 1518
1518 1524
1524 1530
1530 1536
1536 1542
1542 1548
1548 1554
. Opacity
Sum Average
685 30
665 30
625 25
895 35
880 35
955 40
865 35
1025 45
1075 45
770 30
11
12
OVERALL AVERAGE 35
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
!<\V Srorr FnvironmenrA! Technotewv Inc.
-------
#2705-01-0380
-52-
TABLE 34
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Scalping Screen
Test Run No.: 3
Date: 12-8-79
Color of Plume: White
Stack Height: MA
Distance to
Wind Direction:
Sky Description:
Set
Number
1
2
3
4
5
6
7
8
9
10
Time Opacity
Start End Sum Average
1600 1606 690 30
1606 1612 765 30
1612 1618 875 35
1618 1624 555 25
1624 1630 475 20
1630 1636 640 25
1636 1642 500 20
1642 1648 595 25
1648 1654 575 25
1654 1700 610 25
11
12
OVERALL AVERAGE 25
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Scott Environmental Technology !nc
-------
12705-01-0380
-53-
TABLE 35
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Baghouse Bin #1 Outlet
Test Run No.: 1
Date: 12-8-79
Color of Plume: White
Stack Height: so1
Distance to Stack: 150'
Wind Direction:
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
Time , Opacity
Start End Sum Average
1523 1529 55 0
1529 1535 130 5
1535 1541 125 5
1541 1547 130 5
1552 1558 125 5
1558 1604 145 5
1604 1610 150 5
1610 1616 135 5
1616 1622 110 5
10
11
OVERALL AVERAGE 5
12
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
,< \V
-------
12705-01-0380
-54-
TABLE 36
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Baghouse Bin #1 Outlet
Test Run No.: 2
Date: 12-8-79
Color of Plume: White
Stack Height:50'
Distance to Stack: 150'
Wind Direction: N 0-10 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Time Opacity
Start End Sum Average
1626
1632
1638
1644
0900
0906
0912
0918
0924
0930
1345
1351
1357
1403
1409
1422
1428
1632
1638
1644
1650
0906
0912
0918
0924
0930
0936
1351
1357
1403
1409-
1415
1428
1434
175
160
180
125
205
160
165
160
175
115
190
155
60
70
120
150
145
5
5
10
5
10
5
5
5
5
5
10
5
0
5
5
5
5
18
19
OVERALL
AVERAGE
5
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
IIS)1 Scott Environrnentf ITechndcxzv ine
-------
#2705-01-0380
-55-
TABLE 37
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Baghouse Bin #1 Outlet
Test Run No.: 3
Date: 12-9-79
Color of Plume: White
Stack Height: 50'
Distance to Stack:150
Wind Direction: None
Sky Description: High Scattered
Clouds
Set
Number
1
2
3
4
5
6
7
8
9
10
Time Opacity
Start End Sum Average
0942 0948 155 5
0948 0954 115 5
0954 1000 130 5
1000 1006 185 10
1006 1012 200 10
1019 1025 170 5
1025 1031 140 5
1031 1037 155 5
1037 1043 155 5
1043 1049 150 5
11
12
OVERALL AVERAGE 5
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
/T\;
tr •-»*
-------
12705-01-0380
-56-
TABLE 38
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Baghouse Bin 13 Outlet
Test Run No.: 1
Date: 12-5-79
Color of Plume: Whl"te
Stack Height: 12'
Distance to Stack: 25'
Wind Direction: West 5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time Opacity
Start End Sum Average
0835 0841 0 0
0847 0853 60 0
0853 0859 5 0
0859 0905 50 0
0905 0911 90 5
0940 0946 80 5
0946 0952 95 5
0952 0958 115 5
0958 1004 120 5
1004 1010 135 5
11
12
OVERALL AVERAGE 5
13
14
15
16
17
18
19
r r n i *•
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
j{Sj! Scotr Environment.\l Technology Inc
-------
#2705-01-0380
_57-
TABLE 39
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Baghouse Bin #3 Outlet
Test Run No.: 2
Date: 12-5-79
Color of Plume: White
Stack Height: 12'
Distance to Stack: 25'
Wind Direction: West 5mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End Sum
1015 1021 20
1021 1027 15
1027 1033 20
1033 1039 25
1039 1045 70
1051 1057 50
1057 1103 75
1103 1109 60
1109 1115 60
1115 1121 60
Opacity
Average
0
0
0
0
5
0
5
0
0
0
11
12
OVERALL AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Scott Environmental TechnoJoqv
-------
#2705-01-0380
-58-
TABLE 40
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Baghouse Bin #3 Outlet
Test Run No.: 3
Date: 12-5-79
Color of Plume: White
Stack Height: 12'
Distance to Stack: 25'
Wind Direction: West 5 mph
Sky Description: Clear
Set Time Opacity
Number Start End Sum Average
1 1134 1140 140 5
2 1140 1146 170 5
3 1146 1153 135 5
4
5 OVERALL AVERAGE 5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
_ 39
40
-------
12705-01-0380 _59~
TABLE 41
SUHKARY OF FUGITIVE EMISSIONS
Date: 12/8/79
Location: Coarse Ore Bin Conveyor Transfer Point
Run No,: " 1
Time Started: . 1146
Time Ended: 1435
Test Duration (seconds): 7200
Cumulative Duration of
Emissions (seconds): 2548
Percentage of Test Duration with
Emissions (%): 35.41
Average (Percent): 35.4%
,tV> Scott EnvironmentM Technofofjv Inc.
-------
#2705-01-0380
TABLE 42
SUMMARY OF FUGITIVE EMISSIONS
Date: 12/8/79
Location: Scalping Screen
Run No.: 1
Time Started: 1453
Time Ended: 1703
Test Duration (seconds): 7200
Cumulative Duration of
Emissions (seconds): 7200
Percentage of Test Duration with
Emissions (%): 100%
Average (Percent): 1002
Scon Environmental "lochnokyjy Inc.
-------
#2705-01-0380
TABLE 43
SUMMARY OF FUGITIVE EMISSIONS
Date: 12/5/79
Location: Scalping Screen
Run No.: ' 1
Time Started: 1050
Time Ended: 1205
Test Duration (seconds): 3600
Cumulative Duration of
Emissions (seconds): 3600
Percentage of Test Duration with
Emissions (%): 100%
Average (Percent): 1001
Is) Scott EnvironmentalTechnotexivInc.
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12705-01-0380
-62-
TABLE 44
SUMMARY OF PARTICULATE RESULTS
Grinder Cyclone Inlet
Date:
Time Started;
Time Ended:
Run No;
Gas Flow Rates, (dscfm) :
Actual Gas Flow Rate
(acfm);
Parti cul ate Concentration
(gr/dscf):
Participate Mass Flow
Rate (Ibs/hr);
12-4
1625
1745
1
11770
14250
19.77
1990
12-5
0900"
1030
2
11190
13730
21,93
2100
12-5
1445
1610
3
11060
14180
23.10
2190
:! Scott Environmental Technology Inc
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12705-01-0380
-63-
TABLE 45
SUMMARY OF PARTICIPATE RESULTS
Grinder Scrubber Inlet
Date:
Time Started:
Time Ended:
Run No:
Gas Flow Rates, (dscfm):
Actual Gas Flow Rate
(acfm):
Particulate Concentration
(gr/dscf):
Particulate Mass Flow
Rate (Ibs/hr):
12-4
1640
1750
1
10600
12800
11.45
1040
12-5
0855
1030
2
10910
13010
13.27
1240
12-5
1300
1410
3
10890
13670
3.361
313.5
Sample suspect leak in cracked filter holder discovered at end of test run,
; Scott Environmental Techndogy Inc
-------
12705-01-0380
-64-
TABLE 46
SUMMARY OF PARTICULATE RESULTS
Grinder Scrubber Outlet
Date:
Time Started;
Time Ended:
Run No:
Gas Flow Rates, (dscfm):
Actual Gas Flow Rate
(acfm):
Particulate Concentration
(gr/dscf):
Particulate Mass Flow
Rate (Ibs/hr):
12-5
1314
1418
1
10890
12450
0.0822
7.7
Scott Environmental Technology !nc
-------
12705-01-0380
-65-
TABLE 47
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-5-79 pbar(1n- Hg): 29.89
Time: 2330 oar
Sampling Location: Dry Grinder Cyclone ftac_k T™P- N: "
Traverse Point No. Sampled: 3 Inlet Sample Time (Mm): -50
Run No • 1 SamplG Volume (cf):o'J
Run N°" l Moisture (« HJ3): 2.2
Meter Temperature ( F): 73.0
Flow Setting, AH (in. H?0): 3.1
Nozzle Diameter (In.): -250
Sample Flow Rate (at stack conditions) - .94 cfm
ECD1
(Micrometers)
10.59 and larger
6.75
4.44
3.07
1.96
1.00
.60
.40
O40
Total 329.10
ECD - Effective Cutoff Diameter of preceding plate.
?
Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
224. 402
34.65
28.90
17.45
9.70
9.20
3.30
1.20
.30
%
68.18
10.52
8.78
5.30
2.94
2.79
1.00
.36
.09
Cumulative
%
100.00
31.81
21.28
12.50
7.20
4.25
1.45
.45
.09
Scott Environmental Technofogy Inc.
-------
12705-01-0380
TABLE 48
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-5-79 ^(in. Hg)^ 29.51
Sampiing Location: Dry Grinder Cyclone Inle|^k Temp. ( F): 172.0
Traverse Point No. Sailed: 3 W J M n -K.
Run No': 2 Moisture («H90): n 3.1
Meter Temperature (F): 109-°
Flow Setting, dH (in. H90): 3.10
Nozzle Diameter (In.): ^ -250
Sample Flow Rate (at stack conditions) - 1.71 cfm
Plate Net Wt. Cumulative ECD1
No. (mg) $ % (Micrometers)
1 345.20^ 64.42 100.00 7.79 and larger
2 72.80 13.58 35.57 5.02
3 49.20 9.18 21.99 3.28
4 33.60 6.27 12.81 2.26
5 14.70 2.74 6.54 1.45
6 14.50 2.70 3.79 .73
7 .85 .15 1.09 .43
3 2.80 .52 .93 .28
2.20 -41 .41
Total 535.85
ECD - Effective Cutoff Diameter of preceding plate.
2
Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technology Inc.
-------
#2705-01-0380
-67-
TABLE 49
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-5-79
Time: 2334
Sampl'ing Location: Dry Grinder Cyclone
Traverse Point No. Sampled: 3
Rlin Nn . 3
Run N°"
Pbar(in. Hg): 29.38
Inleftac.k T!mP- { f)- 1JO.O
Sample Time (Mm): .25
Sample Volume cf ) : .246
Moisture (% H?0): 2.5
Meter Temperature ( F): 95.0
Flow Setting, AH (in. H?0) : 3.10
Nozzle Diameter (In.): -250
Sample Flow Rate (at stack conditions) - 1.01 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(mg)
977. 702
122,00
79.10
47.10
35.55
21.40
12.40
3.10
1.30
%
75.22
9.38
6.08
3.62
2.73
1.64
.95
.23
.10
Cumulative
%
100.00
24.77
15.38
9.29
5.67
2.93
1.29
.33
.10
ECD1
(Micrometers )
10.22 and larger
6.52
4.29
2.96
1.89
.96
.58
.38
^,38
Total 1299.65
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technolosy Inc.
-------
rs.fc.ur' f 1.1.
39,99
0.5 0,2 0,1 0.05 0.01
FIGURE 10
DRY GRINDER CYCLONE INLET
RUN 1
RUN 2
RUN 3
0 SI
I ; I j. 1 i i ! * -j -
i i 1 1 1 1 1 1 i !
n Stated
nmjjjir
11!!]'
i JH <
i
1
i
i
"
_
-
"
..
"
•_
_
—
—
— -
—
—
....
_..
—
"
—
—
—
n
i
"
i
i
r
±
!
N
11
Q
— /*\
!!!!
IT
-------
#2705-01-0380
-69-
TABLE 50
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-5-79
Time: 2336
Sampling Location;
Traverse Point No,
Run No.: 1
Sampled: 3
Pbar(in. Hg): 29.90
Dry Grinder Scrubber Stack Temp. ( F): 166.0
Inlet Sample Time (Min): .25
Sample Volume (cf): -170
Moisture (% H20): 2.4
Meter Temperature ( F): 100,0
Flow Setting, AH (in. O): 1.05
Nozzle Diameter (In.): .210
Sample Flow Rate {at stack conditions) - .69 cfm
Plate
No.
1
2
3
4
5
6
7
8
Net Wt
(mg_)
2
93.00
14.00
21.40
9.00
7.60
4.65
2.55
1.90
Back-up
Filter 2-50
59.38
8.93
13.66
5.74
4.85
2.96
1.62
1.21
1.59
Cumulative
%
100.00
40.61
31.67
18.00
12.26
7.40
4.43
2.80
ECO*
(Micrometers )
12.35 and larger
7.82
5.17
3.57
2.28
1.17
.70
.47
1.59
C47
Total 156.60
1
ECD - Effective Cutoff Diameter of preceding plate.
?
"Weight includes participate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environmental Technology Inc.
-------
#2705-01-0380
-70-
TABLE 51
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-5-79
Time: 2338
Sampling Location: Dry Grinder Scrubber
Sampled; 3
Traverse Point No.
Run No.: 2
Pbar(in. Hg): 29.54
Stack Temp. (°F): 166.0
Inlet Sample Time (Min): .25
Sample Volume (cf): .200
Moisture (% H~0); 1.2
Meter Temperature ( F): 98.0
Flow Setting, AH (in. H90): 2.00
Nozzle Diameter (In.): L .250
Sample Flow Rate (at stack conditions) - .81 cfrn
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
(nig)
155. 502
25.70
19.10
12.00
10.35
10.20
3.85
2.10
4.10
64.01
10.58
7.86
4.94
4.26
4.19
1.58
.86
1.68
Cumulative
%
100.00
35.98
25.40
17.53
12.59
8.33
4.13
2.55
ECDA
(Micrometers }
11.43 and larger
7.26
4.79
3.31
2.11
1.08
.65
.43
1.68
^..43
Total 242.90
1
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
Scott Environment*! Technology inc.
-------
12705-01-0380
-71-
TABLE 52
PARTICLE SIZE DISTRIBUTION ANALYSIS
Date: 12-5-79
Time: 1240
Sampling Location: Dry Grinder Scrubber
Traverse Point No. Sampled: 3 Inlet
Run No.: 3
Pbar,(in. Hg): 29.40
Stack Temp. (°F): 179.0
Sample Time (Min): .25
Sample Volume (cf): .547
Moisture (% H?0): 2.4
Meter Temperature ( F): 98.0
Flow Setting, AH (in. H90): 2.00
Nozzle Diameter (In.): .250
Sample Flow Rate (at stack conditions) - 2.24 cfm
Plate
No.
1
2
3
4
5
6
7
8
Back-up
Filter
Net Wt.
135. 802
22.50
7.90
4.75
2.75
3.30
1.10
3.40
9.60
%
71.06
11.77
4.13
2.48
1.43
1.72
.57
1.77
5.02
Cumulative
100.00
28.93
17.16
13.02
10.54
9.10
7.37
6.80
5.02
ECD1
(Hicrometers )
6,81 and larger
4.40
2.87 '
•1.98
1.27
.63
.37
.24
^.24
Total
ECD - Effective Cutoff Diameter of preceding plate.
"Weight includes particulate collected on Plate No. 0 and in nozzle and
head of sampler upstream of the collection plates.
\f\}! Scott Environmental Technology Inc.
-------
ift.n
1 0.5 0.? 0,1 0.03 0.01 .
70 60 50 <0 30 20
FIGURE 11
DRY GRINDER SCRUBBER INLET
RUN 1
Cumulative %, Less Than Stated
Particle Size
-------
#2705-01-0380
-73-
TABLE 53
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Grinder Conveyor Inlet
Test Run No.: 1
Date: 12-4-79
Color of Plume: White
Stack Height: NA
Distance to Stack: 12'
Wind Direction:NA
Sky Description:NA
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
•16
17
18
19
20
Time
Start End
1631
1637
1643
1649
1655
1701
1707
1713
1719
1725
1731
1737
1743
1749
1755
1801
1807
1813
1819
1825
1637
1643
1649
1655
1701
1707
1713
1719
1725
1731
1737
1743
1749
1755
1801
1807
1813
1819
1825
1831
Opacity
Sum Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
- 0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
. o
0
0
Set Time - Opacity
Number Start End Sum Averaae
21 1831 1837
22
23 OVERALL AVERAGE 0
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
' Scott Environmental Techndosy Inc
-------
12705-01-0380
_74-
TABLE 54
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Grinder Conveyor Inlet
Test Run No.: 2
Date: 12-5-79
Color of Plume: White
Stack Height: 4'
Distance to Stack: 15'
Wind Direction: Indoors
Sky Description: NA
Set Time Opacity
Number Start End Sum Average
1 0958 1004 0 0
2 1004 1010 0 0
3 1010 1016 0 0
4 1016 1022 0 0
5 1022 1028 0 0
6 1028 1034 0 0
7 1034 1040 0 0
8
g OVERALL AVERAGE 0
10
11
12
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
22 .
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
...39 _.. .
40
Scott Environmental Tvr.hndozylnc
-------
#2705-01-0380
-75-
TABLE 55
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Grinder Conveyor
Test Run No.: 3
Date: 12-5-79
Color of Plume: White
Hood Height: 4'
Distance to Stack:15'
Wind Direction: NA
Sky Description: Indoors
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
1330 1336
1336 1342
1342 1348
1348 1354
1354 1400
1400 1406
1406 1412
1412 1418
1418 1424
1424 1430
Opaci ty
Sum Average
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
11
12
OVERALL AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
21
. 22 „.
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Scott Environmental "Sxhnob^y Inc
-------
12705-01-0380 -76-
TABLE 56
SUMMARY OF FUGITIVE EMISSIONS
Date: 12/4/79 . 12/5/79 12/5/79
Location: Grinder Conveyor Inlet
Run No.: 1 2 3
Time Started: 1628 1313 0856
Time Ended: 1840 1512 1041
Test Duration (seconds): 6055 4500 _ 4380
Cumulative Duration of
Emissions (seconds): 0 00
Percentage of Test Duration with
Emissions (%): 0 00
Average (Percent): 0
Scott Environmental Technology Inc.
-------
#2705-01-0380
-77-
TABLE 57
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Grinder Scrubber Outlet
Test Run No.: 1
Date: 12-5-79
Color of Plume: White
Stack Height: 125'
Distance to Stack: 100'
Wind Direction: SW 0-5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time Opacity
Start End Sum Average
1315 1321 600 25
2321 1327 560 25
1327 1333 540 20
1333 1339 530 20
1339 1345 550 25
1345 1351 555 25
1351 1357 555 25
1357 1403 545 25
1403 1409 545 25
1409 1415 550 25
11
12
OVERALL AVERAGE 25
13
14
15
16
17
18
19
,„ , t
20
Set Time Opacity
Number Start End Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
' Scott Environmenial"fechndo2y!nc
-------
12705-01-0380 -78-
As a result of only one participate being conducted on the scrubber
outlet, no attempt was made to determine scrubber efficiency,
3.4 FINE ORE BIN AND TAILINGS POND
Visible emissions were monitored at the fine ore bin baghouse outlet
using EPA Method 19. Results are summarized in Tables 58 through 60. Visible
emissions at the tailings pond were monitored using both EPA Method #9 and #22.
Results are summarized in Tables 61 through 63 for Method #9 (opacity) and
Table 64 for Method #22 (fugitive emissons). Field data sheets are shown in
Appendix D.
3.5 TRACE ELEMENT ANALYSIS
Particulate samples from two Method #5 tests were subjected to an
analysis for trace elements. Results of the analyses conducted are presented
in Appendix G. The samples analyzed are as follows:
o Grinder Cyclone Inlet, Run 12
- Sample 137689
o Dryer Cyclone Inlet North, Run 14
- Sample 137691
Scott Environmental Technology inc.
-------
#2705-01-0380
_79-
TABLE 58
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Fine Ore Bin, Baghouse Outlet
Test Run No.: 1
Date: 12-7-79
Color of Plume: White
Stack Height: 4'
Distance to Stack: 20'
Wind Direction: West 0-5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time Opacity
Start End Sum Average
1350
1356
1402
1408
1414
1420
1426
1432
1438
1444
1356 60 0
1402 55 0
1408 45 0
1414 40
1420 35 0
1426 20 0
1432 30 0
1438 30 0
1444 40 0
1450 20 0
11
12
OVERALL
AVERAGE 0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sum Averaae
..21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
' Scott Environmental Technokyjy Inc
-------
12705-01-0380
-80-
TABLE 59
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Fine Ore Bin, Baghouse Outlet
Test Run No,: 2
Date: 12-7-70
Color of Plume: White
Stack Height: 4' above roof
Distance to Stack:20
Hind Direction: N/W 5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time Opacity
Start End Sura Average
1515 1521 25 0
1521 1527 0 0
1527 1533 25 0
1533 1539 25 0
1539 1545 20 0
1545 1551 15 0
1551 1557 15 0
1557 1603 10 0
1603 1609 30 0
1609 1615 45 0
11
12
OVERALL AVERAGE 0
13
14
15
16
17
18
19
20
Set Time . Opacity
Number Start End 'Sum Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
' Scott Environmental Technology Inc
-------
#2705-01-0380
-81-
TABLE 60
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Fine Ore Bin-Baghouse Outlet
Test Run No.: 3
Date: 12-7-79
Color of Plume: White
Stack Height: 4'
Distance to Stack:20'
Wind Direction:NW 5 mph
Sky Description:Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
1615 1621
1621 1627
1627 1633
1633 1639
1639 1645
1645 1651
1651 1657
1657 1703
1703 1709
1709 1715
Opacity
Sum Average
35 0
20 0
20 0
15 0
15 0
25 0
30 0
35 0
20 0
50 0
11
12
OVERALL AVERAGE
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End "Sum ' Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Scott Environmental Technology inc
-------
#2705-01-0380
-82-
TABLE 61
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Tailing Pond
Test Run No.: 1
Date: 12-6-79
Color of Plume: White
Stack Height: NA
Distance to Stack: NA
Mind Direction: West 0-5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End Sum
0857 0903 0
0903 0909 0
0909 0915 0
0915 0921 0
0921 0927 0
0927 0933 0
0933 0939 0
0939 0945 0
0945 0951 0
0951 0957 0
Opacity
Average
0
0
0
0
0
0
0
0
0
0
11
12
OVERALL AVERAGE
0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End "Sura Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
i{\); Scott Environmental Tethndoiy Inc.
-------
#2705-01-0380
-33-
TABLE 62
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Tailing Pond
Test Run No.: 2
Date: 12-6-79
Color of Plume; White
Stack Height: NA
Distance to Stack: NA
Wind Direction: West 5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
1010 1016
1016 1022
1022 1028
1028 1034
1034 1040
1040 1046
1046 1052
1052 1058
1058 1104
1104 1110
. Opacity
Sum Average
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
0 0
H
12
OVERALL AVERAGE 0
13
14
15
16
17
18
19
20
Set Tirae Opacity
Number Start End Sum Averaoe
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
;! Scott Environments I Technology Ire.
-------
12705-01-0380
-34-
TABLE 63
SUMMARY OF RESULTS OF OPACITY READINGS
Location: Tailing Pond
Test Run No,: 3
Date: 12-6-79
Color of Plume: White
Stack Height: fj/\
Distance to Stack: NA
Wind Direction: West 5 mph
Sky Description: Clear
Set
Number
1
2
3
4
5
6
7
8
9
10
Time
Start End
1120
1126
1132
1138
1144
1150
1156
1202
1208
1214
1126
1132
1138
1144
1150
1156
1202
1208
1214
1220
Opacity
Sum Average
0 0
0 0
0 0
0 0
0 0
10 0
25 0
55 0
145 5
115 5
11
12
OVERALL
AVERAGE 0
13
14
15
16
17
18
19
20
Set Time Opacity
Number Start End Sura Averaae
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
l{\}; Scott Environmental Technobgy Inc.
-------
12705-01-0380 _85-
TABLE 64
SUMMARY OF FUGITIVE EMISSIONS
Date: 12/6/79
Location: Tailings Pond
Run No.: • 1
Time Started: 0857
Time Ended: 1220
Test Duration (seconds): 10800
Cumulative Duration of
Emissions (seconds): 990
Percentaae of Test Duration with
Emissions (%}: 9-2%
Average (Percent): 9.2%
Scott Environmental Technology Inc.
-------
12705-01-0380 -86-
4.0 SAMPLING AND ANALYTICAL PROCEDURES
Presented in this section is a summary of sampling and analytical
procedures used during testing. For further details the reader is referred to
the description of each EPA Reference Method published in the "Standards of
Performance for New Stationary Sources", Appendix A, Federa1 Regj s ter, Volume 42,
No. 160, Thursday, August 18, 1977, PP 4175588.
4.1 SAMPLING PROCEDURES
4.1.1 Sjejjiction of Sampling Location - EPA Method II
The sampling locations were selected in accordance with EPA Method #1.
This method requires that the sampling location be a minimum of two stack
diameters downstream and a half a diameter upstream from any flow disturbances.
This method also allows the smallest stack diameter to be 12 inches. For
rectangular ducts, an equivalent duct size is calculated. The number of sampling
points is specified in the method, depending upon the length of undisturbed flow
upstream and downstream from the sampling location. The number of sampling points
varies from eight to forty-eight.
Each sampling location was selected so as to provide the maximum length
of undisturbed flow upstream and downstream from the sampling locations and, thus,
the minimum number of required sampling points. The number of sampling points at
each location was then selected based on EPA Method II criteria.
o Coarse Ore Drier - Figure 1 presents a description of the two cyclone
and two wet scrubber inlets and one outlet sampling locations associated with the
drier. A description of the inlet and outlet sampling points are presented in
Figure 12.
o Coarse Ore Grinder - Figure 3 presents a description of the cyclone
and wet scrubber inlets and one outlet associated with the coarse ore grinder.
A description of the inlet and outlet sampling points are presented in Figure 13.
4.1.2 Measurement of Gas Volume Flow Rate - EPA Method #2
The gas volume flow rate was measured at each sampling location in
accordance with EPA Method #2. This method uses a Type S Pitot tube and an
inclined manometer to measure the velocity pressure, and a thermocouple to
measure gas temperature at each sampling point.
Preliminary velocity measurements were made at each sampling location
followed by velocity measurements as a part of each particulate test run.
The Pitot tubes used are within the dimensional limitations of Method
#2. A calibration factor from 0.834 to 0.838 was used for the Pitots.
Scott Environmental ,r:chnoto3y I^
-------
;2705-G1-038Q
-87-
Cyclone Inlet
North
-4"
.-2"
7
ro
ID
Cyclone Inlet
South
L_
o
o
o
OJ
1
7
o
o
o
•8
/ c*
l~J •
/ ot
_ 3
Scruooar Inlot
Scrubber Inlet
Scrubber Outlet
' /
i
2"
4" L
2"
' r
T
^^ I
<
i
7
' 2"
-4" L
...2"
1 '
U3
1
C--T
/
^
1-
° /
O ^>
O
1 . ' '
* . J
0> /
-7 . d-
/ m
/ eg
JL
° )
7O^
1 °
.»
CTl
7-
/ CNJ
JL
Sampling
1
2
3
4
5
6
Point Wall (Inc
3.70
12.26
24.86
59.14
71.74
80.30
FIGURE 12 - COARSE ORE DRIER
Scott Environment \\ Technology Inc.
-------
Cyclone Inlet
Scrubber Inlet
Scrubber Outlet
Sample Points:
1 1.32
2 4.38
3 8.88
4 21.12
5 25.62
6 28.68
Sample Points:
1 1.32
2 4.38
3 8.88
4 21.12
5 25.62
6 28.68
no
o
tn
o
tu
CO
o
1
eo
oo
i
FIGURE 13
COARSE ORE GRINDER SAMPLING POINTS
-------
#2705-01-0330 -89-
4.1.3 Average Stack Gas Molecu!a^ Wei ght - JEPA Method 13
The average molecular v/eight of the stack gas during each test at
the drier was determined by Orsat analysis for CO^ and CL content of the stack
gas in accordance with EPA Method #4. A molecular v/eight of 28.84 v/as used at
the grinder since the process does not involve combustion.
4,1.4 Peterniination of Jtack Gas^Jjoisture Content - EPA Method 14
Moisture content of the gases sampled was determined in accordance
with EPA Method #4 as part of the participate sampling train. F^loisture in the
gas sampled was collected irt impingers in an ice bath followed by silica gel.
The moisture collected was then measured volumetrically and gravimetrically.
4.1.5 Petermina ti on of Par t i c u 1 ate Emi ssigns - EPA Met hod $5
* -_--."
Parti cut! ate emissions were measured in accordance with EPA Method #5.
This method involves the isokinetic extraction of a sample from the gas stream
and collection of the particulate on a heated out-of-stack filter. A dry gas
meter measures the volume of the gas sample. Figure 14 shows a diagram of the
sampling train.
4.1.6 DeterminationofParticle Size - Andersen Cascade Impactor
The samples for particle size distribution at each sampling location
were collected using an Andersen 2000 cascade impactor. The particles are
collected by impaction on a series of plates. The plates have increasingly
smaller holes so that the velocity of the particles is increased from plate to
plate, and smaller and smaller particles are impacted. The particulate weight
collected on each plate is determined gravimetrically. The particle size
distribution is based on the equivalent aerodynamic size of the particles based
on spherical particles of I gratn/cc density.
Sampling and calculations of results were performed in accordance with
the operating manual published by Andersen 2000. Figure 15 shows a diagram of
the sampling train. The impactor was used out-of-stack at the inlet sampling
locations due to the small diameter of these ducts. For this arrangement, a
short probe was installed between the nozzle and cascade impactor.
4.1.7 Determination of Visible Emissions - EPA Method 19
Visible emissions were monitored by determining the smoke density using
EPA Method 19. This method involves the measurement of smoke density by a smoke
reader who has been previously certified against smoke measured by an opacity
meter calibrated with neutral density filters.
Scott Environmental Technology Inc.
-------
rsj
o
01
o
o
CO
CO
o
LEGEND;
1. NOZZLE
2. PROBE
3. PITOT
4. THERMOCOUPLE
5. PYROMETER
6. INCLINE MANOMETER
7, CYCLONE
8. FLASK
9. FILTER ASSEMBLY
10. FILTER BOX
11. IMPINGER ICEBATH
12. IMPIM6ERS
13. THERMOMETER
-.14. CHECK VALVE
15. UMBILICAL CORD
16. VACUUM GAUGE
FIGURE 14 - PARTICULATE SAMPLING TRAIN
17. COARSE FLOW ADJUST
VALVE
18, FINE FLOW ADJUST
VALVE
19. VACUUM PUMP
20. DRY TEST METER
21. ORIFICE TUBE
22. SOLENOID VALVES
-------
o
tr
8
Jl
\
1 1
F^ V
i
o
i
o
CO
o
LEGEND,:
1. NOZZLE
2. PROBE
3. ANDERSEN CASCADE IMPACTOR
4. INCLINE MANOMETER
5. IMPINGER ICEBATH
6. IHPINGERS
7. THERMOMETER
8. CHECK VALVE
9. UMBILICAL CORD
10; VACUUM GAUGE
11. COARSE FLOW ADJUST
' VALVE
12. FINE FLOW ADJUST
VALVE
13. VACUUM PUMP
14. DRY TEST METER
15. ORIFICE TUBE
16. SOLENOID VALVES
FIGURE IB - PARTICLE SIZE DISTRIBUTION SAMPLING TRAIN
-------
12705-01-0380 -92-
4.1.8 Detertinnation of Fu9itivg__EmissiQns from Material Processing Source_s
EPA proposed Method #22 determines the amount of time that any visible
emissions occur during the observation period-, i.e., the accumulated emission
time. This method does not require that the opacity of emissions be determined.
Since this procedure requires only the determination of whether a visible
emission occurs and does not require the determination of opacity levels,
observer certification according to the procedures of Reference Test Method 19
are not required.
4.2 ANALYTICAL PROCEDURES
4-2.1 Paniculate Emissions - EPA Method #5
Particulate emissions were determined gravimetrically in accordance
with EPA Method #5. Prior to testing, absolute participate filters were
dessicated, weighed and sealed in a container for transporting. Upon completion
of field testing, each filter was dessicated and reweighed to determine the
amount of particulate collected.
4.2.2 P a r t i c u 1 ajte_ __Sijz e - A nd e r s en Cascade Imp a c tor
Particulate size distributions were determined gravimetrically using
Andersen cascade impactor substrates. Each substrate was prepared and analyzed
using a method identical to that described for EPA Method #5 particulate
filters.
Scott Environmental Technology Inc
-------
#2705-01-0380 -93-
APPENDIX A
COMPLETE PARTICULATE RESULTS
INCLUDING
FORMULAS USED IN CALCULATIONS
Scott Environmental Technology Inc.
-------
Location: .94.
Grinder
Cyclone Inlet
Grinder
Scrubber Inlet
r^/uo-ui-ujBu _ -
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: P. (in. Hg.)
Static Pressure: P (in. HJ))
Area of Stack: A (ft2)
Pilot Coefficient: C
J " " " j
Keter Calibration- Factor: Y
Area of Nozzle: An (in2)
Total Sampling Time: "(Min.)
Gas Sample Volume: Vm (ft*)
n
Avg. Velocity Head: (VTp ")avg. (in. O)
Avg. Orifice Pressure: AH (in O)
Avg. Stack Temperature: T (°R)
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: Vj (ml.)
Gas Sample Volume 0 Std. Cond.:
Ysn(Std) (ft3) = 17.64 Vrr.Y (P^ +AH/13.6)
Tm bar
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 Vj
Moisture Content: B ="" Yw(Std)
** • Vm(Std) + Vw(Std)
ftolecular Weiaht of Stack Gas (dry):
Hd * 0.44 (f C02) - 0.32 (% Og) +
0.28 (% N9+* CO)
c \
1
12-4
t.^™,,
1625 j
121£__
29.89
4.8
4,91
0.834
1.00
0.0491
60
43.634
0.63
2.19
632
563
20
41.082
0.94
0.022
28.84
2
12-jj j]
0900
1030
29.51
4,8
4.91
0,834
1.00
0.0491
60
50.723
0,58
2.4 .
627
557
32
47.688
1.51
0.031
28.84
3
L2-5
L445
1610
?9.38
4.8
4.91
0.834
1.00
0.0491
60
49,428
0.59
2.5
656
570
25
45.223
1.18
0.025
28.84
1
12-4
1640
1750
29.90
2.5
4.91
0.834
1,00
0.0491
52.25
39.84
0.51
1.8
626
548
20
38.515
0.94
.UcH
28.84
2
12-5
0855
1030
29.54
2.5
4.91 •
0.834
1.00
0.0346
60
35.33
0.53
1.0
618
542
9
34.051
0.42
n ni 9
U. Ul£
28.84
3
12-5
1300
1410
29,40
2.5
4.91
0.834
1.00
0.034C
60
38.467
0.56
1.1
639
558
19
35.85C
0.89
n n?d
28.84
Scott
-------
12705-01-0380
Folecular Weight of
Stack Pressure: P
-95-
Location
Run Number
Stack Gas (wet):
{in' H9} = Pbar 4 V13"6
Stack Gas Velocity: 1/2
v (ft/sec) = 85.49 C UPTS/P$!V
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 (!-BWS)VS A PS/T$
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v A
Weight of Particulate Collected: m (mg.)
Concentration of Particulate E? Std.Cond.(dry):
C (gr/scf) = 0.01542 m /V (std)
C: (g/dscm) = 0.03529 m /V (std)
Mass Flow Rate of Particulate:
Q (Ib/hr) - 0.003571 GS Q$d
Jsokinetic Rate:
1 (*)• 13.61 TsVm(std)/PsvsAne(l-8ws)
Grinder
u Cyclone Inlet
r
28.60
30.24
48.38
11770
14250
52682.
19.77
1990
83.9
2
28.51
>9.86
16.60
11190
13730
67819.
21.93
2100
102.4
3
28.57
29.73
48.13
11060
14180
67750
23.10
2190
98.3
Grinder
Scrubber Inlet
1
28.58
30.08
43.45
1
10600
12800
28605. £
11.45
1040
100.25
2
28,71
29.72
44,17
10910
13010
29296.5
13.27
1240
106.4
3
28.58
29.58
46.39
10890
13670
7806-;
3.36"
313. b
112.2
* Sample suspect. Leak in cracked filter holder discovered at end of test run,
-------
Location; -96-
Grinder Scrubber
..Outlet
#i:/ub-ui-u,s5u
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: P^ (in. Hg.)
Static Pressure: P (in. H?0)
Area of Stack: A (ft2)
Pi tot Coefficient: C
P
Keter Calibration- Factor: Y
2
Area of Nozzle: An (in )
Total Sampling Time: ^{Min,}
Gas Sample Volume: Ym {ft )
Avg. Velocity Head: (VrTp"~)3vg, (in, HJD)
Avg, Orifice Pressure: AH (in HJ))
Avg. Stack Temperature: T (°R)
»J
Avg, Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: V (ml.)
Gas Sample Volume @ Std. Cond.:
Vm(Std) (ft3) = 17.64 VmY (?k +tH/13.6)
Tm bar
Yolu-T.e of Water Vapor:
Yw (std) (ft3) = 0.04707 Vlc
Moisture Content: B *' Vw(Std)
w" • Ym(Std) T Vw(Std)
ffelecular Weicht of Stack Gas (dry):
Hd - 0.44 (5f C02) 4- 0.32 (% 0^) +
0.28 {% M2+S CO)
1
12-5-79
1314
1418
29.40
0.30
7.07
0.834
1.00
0.0491
60
35.254
0.25
1.06
565
539
37
34.011
1.74
.u4y
28.84
.
(\l Scot?F.nvirnnmenfA!TechnokwvInc.
-------
12705-01-0380
-97-
Location
Run Number
Grinder
>crubber
Jutlet
1
folecular Height of Stack Gas (v/et);
Hs - Md (1-BWS) + 18.0 Bws
28.31
Stack Pressure: P (in. Hg) = P, + P /13.6
29.42
Stack Gas Velocity:
v (ft/sec) = 85.49 C
1/2
29.36
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 (I-BWS)VS A PS/TS
10890
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v A
12450
Weight of Particulate Collected: m (nig.)
181.4
Concentration of Particulate @ Std.Cond.(dry)
Cc (gr/scf) = 0.01542 m/Vn (std)
C (g/dscrn) = 0.03529 m/V (std)
0.0822
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.008571 C Q d
7.7
Isokinetic Rate:
I (S). 13.61 T5Vm(std)/PsvsAn9(l-Bws)
108.0
Control Efficiency, %
-------
Drier
. Location: -98- f-in^th rvrlone Inlet
jiTinc m noon -7tJ '"•*' ^li i'Vv-i«Jiic initi. .
#2705-Ql-03ou
Run Number;
Date:
Tiii}2 Started:
Time Ended:
Barometric Pressure: P. (in. Hg.)
Static Pressure: P (in. H^O)
Area of Stack: A (ft2)
Mtot Coefficient: C
Meter Calibration -Factor: Y
2
Area of Nozzle: An (in )
Total Sampling Time: ^(Min.)
Gas Sample Volume: Vm (ft3)
Avg. Velocity Head: (\Ttp )avg. (in, H20)
Avg. Orifice Pressure: AH (in H?0)
Avg. Stack Temperature: T (°R)
Avg. Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: V, (ml.)
1C
Gas Sarr.pl e Volurce fl Std. Cond,:
Vm(Std) (ft3) = 17.64 Y~Y (P, +AH/13.6)
Tm Ur
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 Y^
Moisture Content: B ^ ='" Vw(Std)
Hj • Vm(Std) + Yw(Std)
Hoi ecu! a r Weicht of Stack Gas (dry):
Md = 0.44 (S" C02) + 0.32 (% ^} i-
0.28 (% H2+S CO)
4
ii±,,l:
1924
i
29.48
-0.16
13.1
0.834
1.00
0,1104
82
33.028
D.28
2.5
757
519
515
63.547
24.24
0.276
29". 18
5
•*«*
-------
99-
12*705-01-0380
Location
Run Number
Molecular Weight of Stack Gas (wet):
Ks*Md(l-BHS) + 18.0Bw5
Stack Pressure: PS (in. Hg) = Pfaar 4 P /13.6
Stack Gas Velocity: 1/2
vfi (ft/sec) = 85.49 Cp (APT$/PSMS)
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 {l-Bws)v$ A P$/TS
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 vg A
Weight of Participate Collected: m (mg.)
Concentration of Participate @ Std.Cond.(dry)
C. (gr/scf) = 0.01542 m /V (std)
C* (g/dscm) = 0.03529 mJj/VJJ (std)
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.003571 C$ Qsd
Isokinetic Rate:
I (%) = 13.61 Ts Vm(std)/PsvsAn0(l-Bws}
Drier
North Cyclone Inlet
4'
26.09
29.47
37.43
14630
29420
214330
52.01
6520
90.6
5
25.72
29.69
26.80
11300
21060
89050
87.23
8450
108.3
6
26.22
30.16
28.20
11220
22160
142740
99.64
9580
112.2
7
26.15
30.13
35.93
13680
28240
120780
71.54
8390
101.7
.M*.
-------
Drier
' #2*705-01-0380 ; Location: _100_
Run Number:
i - Date:
Time Started:
Time Ended:
Barometric Pressure: Pbar (in. Hg.)
Static Pressure: P (in. HJ))
Area of Stack: A (ft2)
Pilot Coefficient: C
Keter Calibration- Factor: Y
2
Area of Nozzle: An (in )
Total Sampling Time: ^(Hin.)
Gas Sample Volume: Vm {ft3}
Avg. Velocity Head: (fTfT^lvg. (in. H20)
Avg. Orifice Pressure: AH (in FLO)
Avg. Stack Temperature: T (°R)
Avg, Meter Temperature: T (°R)
Volume of Liquid and Silica" Gel
Collected: V (ml.)
Gas Sarr.pl e Volume @ Std. Cond,:
Yro(Std) (ft3) = 17.64 Y~Y (Pk +iH/13.6)
Tm bar
Volume of Water Vapor:
Vw (sld) (ft3) = 0.04707 Yj
Poisture Content: 8., - " Vw(Std)
Wj . Vm(Std) + Vw{Std)
Molecular Weicht of Stack Gas (dry):
Kd = 0.44 (f CQ£) + 0,32 (X 0£) +
0,28 (% N2+S CO)
S.out,b £jt
4, I
12-6
1839
29.48
-0.63
13.3
0.834
1,00
0.110
40
46.43
0.17
1.92
744
623
251
46.387
11.81
0.203
29.06
-LLOJ^fi—Lplet
5
6
12-7 I 12-0
29.70
-0.63
13.3
0.834
1.00
0.110
24
17.105
0.23
1.9
661
531
138
16.956
6.50
0.277
29,06
30.17
-0.63
13.3
0.834
1.00
0.110
32
26.157
0.20
2.2
859
513
209
27.281
9.84
0.265
29.06
7
12-8
30.14
-0.63
13.3
0 . 834
1.00
0.110
32
28.486
0.27
3.2
688
512
298
29.811
14,03
0.320
29.06
-------
12*705-01-0380
-101-
Location
Run Number
Drier
.South Cyclone Inlet
4
Molecular Weight of Stack Gas (wet):
H
B
«s
26.81
26.00
26.13 25.52
Stack Pressure: P^ (in. Hg) = P,
S D3F
P A3.6
29.43 29.65 30.12
30.09
Stack Gas Velocity: 1/2
vs (ft/sec) « 85.49 Cp (&PTS/P$HS)
28.54
31.66
33.10
35.06
Stack Gas Volume Flow Rate:
qsd (dscf /min) = 1059 {I-BWS)VS A PS/TS
12680
14470
12090
14690
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v A
22780
25270 26580
27980
Weight of Particulate Collected: m (mg.)
116590
91760
66553,7
120610
Concentration of Particulate @ Std.Cond.{dry):
C (gr/scf) = 0,01542 m /V (std)
C (g/dscm) = 0.03529 m/v (std)
38.76
83.45
37.62 62.39
Mass Flow Rate of Particulate:
Q (Ib/hr) = 0.008571 C Q
4210
10350
3900
7860
Isokinetic Rate:
I (%) = 13.61 Ts Vm(std)/Ps^Ane(l-Bws)
159.4
85.1
122.9
110.5
-------
Drier
. Location: -in?- North Scrubber Inlet
jin~inr AI m°n A*«- ,_.... . . _._ ,„„
fft/Ub-Ul-UJoU
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: Pbar (in. Hg.)
Static Pressure: P (in, H?0)
Area of Stack: A (ft2)
Pi tot Coefficient: C
Meter Calibration -Factor: Y
p
Area of Nozzle: A (in )
Total Sampling Tirne: ^(Kin.)
- Gas Sample Volume: Vm (ft3)
* Avg. Velocity Head: (VTp )avg. (in. H?0)
Avg. Orifice Pressure: AH (in HJ3)
* Avg, Stack Temperature: T (°R)
Avg, Meter Temperature: T (°R)
Volume of Liquid and Silica' Gel
Collected: Vlc (ml.)
Gas Sample Volume @ Std. Cond.:
Ym(Std) (ft3) = 17.64 Vrr.Y (?k +iH/13.&)
Tm bar
Volume of Water Vapor:
Vw (std) (ft3) = 0.0470? Vlc
Moisture Content: B ='Vw(Std)
w • Vm(Std) r Vw(Std)
Molecular Veicht of Stack Gas (dry):
Hd = 0.44 (f C02) + 0,32 (% 0£) +
0.28 (% \\?+« CO)
4
12-6
1913
2330
29.48
-1.5
13.3
0.834
1.00
0,0716
40
37.032
-
O.ZX/
/o.s;
1.9
781
521
237
37.138
11.16
0.231
29.18
5
12-7
1200
1330
29.70
-1.5
13.3
0.834
1.00
0.0716
20.87
12.476
0.21
1.2
665
528
88
12.415
4.14
0.250
29.18
6
12-8
0930
1035
30.17
-1.5
13.3
0.834
1.00
0.0716
32
21.86
0.2X^
.X0.39
1.6
689/"X
./B59
518
161
22.55
7.58
0.252
29.18
7
12-8
1448
1628
30.14
-1.5
13.3
0.834
1.00
0.0716
32
19.717
xCs5
1.3
589/"
X»31
531
150
19.804
7.06
0.263
29.18
— , — >_.
* Upper figure is average in entire duct.
Lower figure is average at sampling points,
-------
#2*705-01-0380
-103-
Location
Run Number
Drier
North Scrubber Inlet
folecular Weight of Stack Gas (wet):
M
ws
26,60
26.38
26.37
26.24
Stack Pressure: P$ {in. Hg) = P
baf
P /13.6
29.37
29.59
30.06
30.03
* Stack Gas Velocity: 1/2
vs (ft/sec) = 85.49 Cp UPTS/PSMS)
37.0'
40.95
30.16
31.8
/
46.35
31.97
43.32
Stack Gas Yolurr.e Flow Rate:
Qsd (dscf /nin) = 1059 CI-BWS)YS A P$/TS
15090
14170
14660
14470
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v A
29560
24060
25440
25510
Weight of Participate Collected: m (mg.)
19320.
4657.7
9484.3
13372.4
Concentration of Particulate @ Std.Cond.(dry):
C (gr/scf) = 0.01542 m /V (std)
C (g/dscm) = 0.03529 m/v (std)
8.022
5.785
6.486
10.801
Mass Flow Rate of Particulate:
Q (}b/hr) = 0.008571 C Q
1040
703
815
1340
Isokinetic Rate:
10.}- 13.61 TsVm(std)/PsvsAne(l-Bws)
149.0
112.4
110.3
102.0
* Upper figure is average in entire duct.
Lower figure is average at sampling points.
-------
Location:
Drier
South Scrubber Inlet
#£,/UU~Ui~UO-^
xt).35
3.9
748/X
X772
527
221
35.47
10.40
0.227
29.06
5
2-7
1030
1305
29.66
-1.5
13.3
0.834
1.016
0.108
64
60.86
0.27
3.2
675
544
508
59.94
23.91
0.285
29.06
6
12-8
0900
1100
30.17
-1.5
13.3
0.834
1.016
0.108
32
34.825
0.40
4.1
826-
527
132
36.09
6.21
0.147
29.06
7
12-8
1400
1540
30.12
-1,5
13.3
0.834
1.016
0.108
32
28.38
0.30
2.9
759
538
247
28.68
11.63
.288
29.06
* Upper figure is average in entire duct.
-, Lower figure is average at sampling points
-------
#2705-01-0380 . "105~
Location
Run Number
Holecular Weight of Stack Gas (wet):
WI-BKS) + is.o BWS
Stack Pressure: f, (in. Hg) = Ph,_ + PJ13.6
S oar y
Stack Gas Velocity: 1/2
vs (ft/sec) = 85.49 Cp (APTs/PfiHs)
Stack Gas Volume Flow Rate:
Qsd (dscf /min) = 1059 (l-B^ A P$/TS
Actual Stack Gas Volume Flew Rate:
Q (acf /min) = 60 v A
Weight of Particulate Collected: m (tng.)
Concentration of Particulate @ Std.Cond.(dry):
Ce (gr/scf) = 0.01542 m /Vm (std)
Cg (g/dscm) = 0.03529 m[J/V^ (std)
Kass Flow Rate of Particulate:
Q (Ib/hr) = 0.008571 GS Q$d
Isokinetic Rate:
KS)- 13.61 TsVm(std)/PsvsAne(l-Bws)
Drier
South Scrubber Inlet
4*
26.55
29.35
33.5j>x
/tfl.98
14320
26730
25284.1
10.99
1350
106.5
5
25.91
29.55
34.79
15330
27760
36069.5
9.279
1220
108.4
6
27.44
30.06
45.13
19730
J6010
L3993.6
5.979
n- -
pio
L01.4
7
25.87
30.01
38,61
15300
30810
38474.6
20.69
2710
104.0
...
Upper figure is ""average in entire duct.
Lower figure is average at sampling'points.
-------
- Location: 1QA_ iryer Scrubber Outlet
Run Number:
Date:
Time Started:
Time Ended:
Barometric Pressure: Pba (in. Hg.)
Static Pressure: P (in. H?0)
Area of Stack: A (ft2)
Pi tot Coefficient: C
Heter Calibration' Factor: Y
p
Area of Nozzle: A {in )
Total Sampling Time: ^(Hin.)
_Gas Sample Volume: Vm (ft3)
Avg. Velocity Head: (V~Ap )avg. {in. O)
Avg. Orifice Pressure: AH (in HJ3)
Avg. Stack Temperature: T (°R)
Avg, Meter Temperature: T ( R)
Volume of Liquid and Silica' Gel
Collected: V]c (ml.)
Gas Sample Volume Q Std. Cond.;
Ym(Std) (ft3) = 17.64 VrnY (P. +&H/13.6)
Tm
Volume of Water Vapor:
Vw (std) (ft3) = 0.04707 YJc
Moisture Content: B , ="" Vw(Std)
^^ . Vm(Std) T Vw(Std)
hblecular Weight of Stack Gas (dry):
Md = 0.44 (% CCU) + 0.32 (% 0*) +
*" _ £ L*
0.28 (1 H2+2 CO)
(S) Scott Environrriental Technoto^v Inc
4
12-6
1817
2005
29.56
0.0
38.5
0.834
1.00
0.0716
96
51.474
0.19
0.98
619
534
350
50.386
16.47
0.246
28.82
5
12-7
1019
1206
29.72
0.0
38.5
0.834
1.00
0.0716
96
44.936
0.14
0.72
619
529
330
44.613
15.53
0.258
28.82
6
12-8
3828
1029
30.20
0.0
38.5
0.834
1.00
0.0716
96
50.426
0.18
0.97
617
509
347
52.901
16.33
0.236
28.82
1
— .
— __
-.
—
»
-------
107
#2705-01-0380 . "1U/
Location
Run Number
tolecular Weight of Stack Gas (wet):
Hs « Kd (1-BJ + 18.0 Bws
Stack Pressure: P (in. Hg) = P. af + P /13.6
Stack Gas Velocity: 1/2
v$ (ft/sec) = 85.49 C (iPTs/PsHs)
Stack Gas Volurr,e Flow Rate:
Qsd (dscf /rnin) = 1059 (I-BW')VS A PS/T§
Actual Stack Gas Volume Flow Rate:
Q (acf /min) = 60 v$ A
Weight of Particulate Collected: m (mg.)
Concentration of Particulate 0 Std.Cond.(dry):
Cc (gr/scf) = 0,01542 m /V (std)
C* (g/dscrn) = 0.03529 mn/Vra (std)
s n m
Pass Flow Rate of Particulate:
Q (Ib/hr) = 0.003571 C Qsd
Isokinetic Rate:
1 («}« 13.61 TsVm(std)/PsvsAne(l-Bws)
Drier Scrubber
Outlet
4
26.15
29.56
27,81
40800
64240
171.8
0.0526
18.4
99.7
5
6.03
?9.72
23.87
34650
55130
54.2
0.0187
5.6
103.9
6
26.27
30.20
26.68
40680
61630
151.7
0.0442
15.4
105.0
,
—
-------
12705-01-0380 .108-
APPENDIX B
PARTICULATE FIELD DATA SHEETS
Scott Environmental Technology Inc.
-------
PROJECT NUMBER <37oS" TEST NUMBER
FIELD DATA SHEET
ssi
*l TfCMNOLOSr, INC.
1
1-
£
PLANT
DATE
tii.j::>iJ g.M'-ivi^JV' -itrf-^-^ -..-\, PS06E LENGTH S
r-L I «•' ''"•- . . . flOZZt.E 1.0.
SAMPLING LOCATION .
SAMPLE TYPE ?-'-;-
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TYPE 4* ^'.A >5
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C'liti'de1'*'^^' " SA?'iPlE 80X NUMBER -
FYRITE ANALYSIS
C02- °2 __
"--:•. -3" METER BOX NUMBER ScjlfSfc 'A* }. M- .-104.
I PROSE HEATER SETTING
OPERATORS ei*-. •"-T.i. FILTER HEATER
SETTING
WBIEMT TEMPERATURE 1% & \5M< REFERENCE 4? . *£?
BAROMETER ••!.•?
TPAVE8SE
Kt'VEW
1
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NUMU'jlWHWUA BT
T
MOISTURE
WINGERS
FINAL VOLUKE *-**"
INITIAL VOLUME _M£_,
NET VOLUME 4
ANALYTICAL DATA
ACETONE FRONT ^'A5H
FINAL I2%.ift£4
TARE IO4.M41, /
NET tf..t.o f A '
FILTER .NUMBER 1
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SAMPLING TIME (24-hr CLOC*
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GHT DETERMINATION BY _
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-------
PROJECT NUMBER _£
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TEST NUMBER 2-*- FIELD DATA SHEET
PLANT
DATE 1
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SAMPLING LOCATION Cufjiffie. £f;i '{.*+-} » /ff SAMPLE BOX NUMBER - 'TT~''"iA'_
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AMBIENT TEMPERATURE REFHREHCE _P .-*£
BAROMETER Z ~ •>
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-------
.MOISTURE
BPIHSERS
FINAL YCLIBS
HET VOLUME
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SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT ,
NET WEIGHT L5*£L [
»l TOTAL MOISTURE
NOMOGRAPH DATA BY
ANALYTICAL DATA BY
ACETONE FRONT WASH ACETONE SACK WASH
FINAL I0$,3\f»0\ mg FIKAL . "19
TARE 1"f,7laf , mg TARE mg
NET °( , "• ' 7 '., ^ mg NET ' mg
FILTER NUMBER \ ETHER-CHLOROFORM EXTRACT
FINAL ,-S~l3£ mg FINAL rng
TARE.^p* -SS73 , mg TARE mg
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«m*-«U»«ER 2 Afle'-TD^ UJftSHuA-rp* EVAP0P.ATION
FINAL /l/,i-/15S mg FINAL rng
TARE IQ£.%A\"^ • mg TARE • mg
NET £.(>0 ^,5 " mg NET mg
FILTER 'NUMBER 3 A C£r>,'£ tt/A< ft TOTAL BACK rag
FINAL /-V'3, -VS?/ mg , rrs,,c, ,M£T ,k: „.,.„ „ s,,,ltr,
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PROJECT NUMBER ,-TXgl TEST NUMBER _2 FIELD DATA SHEET
PLANT
DATE
LtJ i ° -' o .••- <-• •-••" »'-'sr" "-'"l ' = '" "-* PROSE LENGTH &
r- < "'•'- NOZZLE I.D.
.... •• * -, jO/; SCOTT tNVWONMINTAlTICMNOlOOt. INC
TYPE 31 AUftS-S' "• ' • FYRITE ANALYSIS
• "2.-5O
SAMPLING LOCATION •>-: •-'• .= — t^- -•
SAMPLE TYPE
RUN NUMBER
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NOMOGRAPH DATA BY
_M_QI_$TURE
KPINGERS - 9
FINAL VOLUME g (s o al
INITIAL VOLUXE
BET VOLUKE
ANALYTICAL DATA BY
-114-
SILICA GEL
FINAL WEIGHT 111.
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NOMOGRAPH DATA 8Y
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PRGJECT NUMBER •^li.j" TEST NUMBER :- FIELD DATA SHEET
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PROJECT NUMBER
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-134-
NOMOGRAPH DATA BY
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PROJECT NUMBER - TEST NUMBER
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IELD Di
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NOMOGRAPH DATA BY
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ANALYTICAL DATA BY
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PRCUECT NUMBER ~ " :•.'' TEST NUMBER
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FieLD DATA SHEET
PUNT
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TYPE /C| Jp CETER SOX NUMBER Sr^-H- A ///. ?<5''/ .
RUN NUMBER 7 PROBE HEATER S
R
\
OPERATORS /'
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AMBIENT TEMPERATURE <^» J? *"/-" RE
BAROMETER
1Ii«i'ERSE
2_
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FEREuCE iP
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READ A: D RECORD ALL DATA EVERY 2-~ MINUTES
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JOJSTURE
WPINCERS „ _
FINAL VOLUKE - 6? *7 ;> el
INITIAL VOLUSE J..-"^ »<
HET VOLUKE _JL
~138~
FINAL WEIGHT 3i±L t
ffitTlM. » EIGHT J«. >?•*>. (;
(it f IEIGHT . ....... .-TV"? I
." irl TOTAL WOiSTURE
ANALYTICAL DATA 8Y
ACETONEFRONT WASH
FINAL "j'J .<~t4.'t.
' *i TARE Jji/l±L
NET
FILTERNUMBER1
FINAL /.yilf
TARE
NET
FILTER NUHSER 2
FINAL .-*'-('>
TARE ; j H 2
NET
nLTER.HliMEER 3
FINAL ,/<>. _.'
TARE^Tp ,3ri£fl
'NET' .$ !•-!•••,
CYCLONE
FINAL
TARE
NET
J«9.
_jng
jng
ACETONE BACK »ASH
FIHAL
TARE
NET
mg
_W
rog
jng
jng
mg
ETHER-CHLOROFORM EXTRACT
FINAL mg
TARE mg
NET mg
WATER EVAPORATION
FINAL
TARE mg
NET rog
TOTAL BACK mg
cuiM'Tf c fnKs.fi DIFFI sonui ur oss
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-
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STATIC ntEZUHE 1* ST*CK, •- H|
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d»ER«E VliDCin *LUS. «,. M
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SAMPLING TlVt (24 hr Cl OCIfl
SA.VPl.IN5 LOCATION
jng
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SAMPLE WE iBAG. INTEGRATED,
ANALYTICAL KETHOD
AMBIENT TEKPERATURE___
RUN
TOTAL FRONT \\\''l .
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NVItONMCNTAl TtCHNOlOOlf. INC.
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PROJECT NUMBER
TEST NUMBER-
-139-
FIELD DATA SHEET
• .^PlJNT
GATE
>H CA^IhDg
PROBE LENGTH S TYPE
NOZZLE l.D.
FYRITE ANALYSIS
CO, 0,
SAMPLING
SAMPLE TYPE N£~^Cp ZT_
RUN NUMBER ^"'.^- . •
OPERATORS *T '-^ - M.T
AMBIENT TEMPERATURE
BAROMETER 2«-1
SAMPLE BOX NITOES
KETER BOX NUMBER _
PROSE HEATER SETTIH3 35fff
FILTER HEATER SETTING
REFERENCE iP
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READ AND RECORD ALL DATA EVERY
MINUTES PITOT NUMBER.
TRAVERSSJ ClflCS TSE
P3,,HT S«?UKCJ 1Mb
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2.
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as), it. r.fi
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.MOISTURE
NOMOGRAPH DATA BY
KPiNGERS
FINAL VOLUME H"
INITIAL VOLU?;E_l£
HET VOLUME _j2.
S2b_»i
L2 *t
213=.' «i
5ILIC* GEL
FINAL HEIGHT '
IHfTIAL HEIGHT j
H£T HEIGHT
TOTAL MOISTURE
k6-,.'t
TS . * t
/~n
ANALYTICAL DATA BY
ACEJQNE FROST WASH ACETONE SACK WASH
j ^,-<*-? Wallet* ,&,! Ki9 FINAL «5
X£> TARE -/^ ?V^9 m§ TARE rsg
NET 1 ! Z 9 FINAL mg
TARE -p .^C-.^YN mg TARE mg
.(„•£- "j,ET /£'•?.;'' mg NET mg
FILTER NITOER 2 WATER EVAPORATION
FINAL /. (rt c-7*.~ mg FINAL ng
TARE r3^- ::::li i:r::-: ':-:: ! '::-:;-: rf: Vfi ::-i;: " ':^ri::i!:^''-i ™.:: li:i[i;^:;:' ^:5
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liATIO Of STATIC PRE'Suat 1C tnE« PRESSIKE
»veRKE
TtCKlEi'PLftATORE *F
AVEMSE VELOCr!* KE»J. in. »f
tmxwjt WlCCilY HiAt, m. K^O
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SAMPLING 1 HE IJ4-(ti CLOCK)
SASTLIN:
SAV.PLE 1
ANALYT!
A.V.8IENT
CM
BY
LOCATION
TPE (BA.G, INTEGRATED, CONTIMJOU
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it
TfV.PERATUSE
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PROJECT NUMBER 2/7 05" ........... TEST fluraER
-141-
FIELD DATA SHEET
| SCOTT ENV1KQNMENTAL t
Of , SMC
PLANT VJNMOM C ft.fi. tb\ Q6 PSOBE LENGTH & F'PE & -it. A; I
DATE 12-
*)--(A N02ILE 1
SAMPLING LOCATION
SAHPLE TYPE
RUN NUM3EX
.0.
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C^CLOi4£ -.TfJL^T S«(nw SAMPLE SOX flUMBHR 4f' 2.
FY8ITE ANALYSIS '
co2 oz
M?.-"'.^ /" KETES SOX NUMBER -i*ji_____
2f.lT PROSE HEATER SETTING i-TO'r
OPERATORS 16 Nt-T FILTER HEATER
e
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A'-BIEN
BAROME
TRiVtSSE
PS.ST
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SETTING i5"G-si-'
T TEMPERATURE . REFERENCE iP ,n(*
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5 * i___ * L1"1" rjTLE;J
PITOT NUMBEB _____
1 COMMENTS
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-------
MOISTURE
-142-
NOMOGRAPH DATA BY
WPINGERS
FINAL VOLUSt
INITIAL VCLIW.I
NET VOLUME
3SO
^ l>.^~
ml
ci
si
SILICA GEL
FINAL *• EIGHT
till WEIGHT*
TOTAL OSTLISE
ifejj_t
\"ii •
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I1-'
ANALYTICAL DATA
ACETONE FRONT WASH
FINAL /$ "^ , <*$
TARE C13.')'1^
NET 9/D,//^'"
FILTER fmSER 1
FINAL , i" L- Y I
TARE --7". -T r> •;. •»
NET - d £ r- f
FILTER NUMBER 2 •'
FINAL
TARE
NET
FILTER NUMBER. 3
FINAL
TARE •
NET
<*C-bW£ Woo i
F1KAL C» ^ 2 ^'3
NET ) ,£' | >.^
TOTAL FRONT v\\')\,
SY
mg
• mg
mg
ng
mg
mg
mg
«-'9
mg
ng
«mg
mg
mg
ing
(0 mg
COTT SNVUbNMtNT*!. 1ECMKOIOOV^'N€.
ACETONE BACK WASH
FINAL
TARE
NET
ETHER-CHLOROFORM fXTP
FINAL
TARE'
NET
HATER EVAPORATION
FINAL
TARE
NET
TOTAL BACK
I C'f
E- --^ t,"i s-ir *•'-. f. ^-^-':
scct'-i^»,a v;*r "£Tf.::i CL:, »«
»tp£ ;^ t-: e^Eif?5.::-'. o". \
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Sli'vEC ' &:
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mg
ACT
mg
p>g
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pig
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r.q
fflg
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s-^-'tTr
CUffi'ltED PRE1SMJ Dif f (KKTtU. HSM3J
CH;fCl, us. Hj3
IVEftlaE KTH Tf «?£R»Tl!Rt IMBXKT » R'n.'f
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it STIC THUSOUt IS SHCK. |« H|
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B8TI1CF STUTi: PSWUSC TO ȣTER PRBSJSS
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PROJECT NUMBER
TEST NUMBER
-143-
FIELD DATA SHEET
PUNT
OATE
\J r4 1 O M C, £^' '; -Af.l
•> *! "4T"
T SNVIRQNMENIAt TECHNOLOGY. IKC.
FYRITE ANALYSIS
CO, 0.,
CvCi.ON£" ^M SC^-^r**- SAMPLE BOX NUMBER & "?—
-T^C'% "T^ METER BOX NUMBER -45" -Ji
J£> PR03E HEATER SETTINS
OPERATORS "T^. f-*CT FILTER HEATER
SETTISG
WBIENT TEMPERATURE REFERENCE iP . 1 fa
BAROMETER
BOS! Eft
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ANALYTICAL DATA' BY
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PROJECT NUMBER "2.7 oS TEST NUMBER
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ANALYTICAL DATA BY
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MOISTURE
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NOMOGRAPH DATA BY
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"HffFEREOTUl."1
SESiRt!
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CQmENTS
l_TCf
-------
.MOISTURE
WRINGERS
FINAL VOLUME
INITIAL VOLUV
RET VOLUME
ANALYTICAL DATA BY
-158-
SLICASR
FINAL WEIGHT tLLi±_ I
.MIGHT •s'jfr •"> t
NOMQSRAPH DATA BY
NET WEI3HT
TOTAL KOI5TUHE
; ? . o
ACETONE FRONT WASH ACETONE BACK WASH
FINAL *?/ ."=-£•' — mg FINAL mg
-^•f TARE .nti8F n*Tic pspsast TO KETES pREisaiiE */f.
•VEIl»CEI«WTfrFER»T!iRE.'F t, I
*" "k "' '"' ' "• 2 '"«. |
t.*txft va:an Hia, i«. «z» 4ttJI
C FAtTDR
CHC!.'L/Ifi;ii3:;LLDI»VEUS.».
»C7WLi;3MUC:«EUR.« )
ReF™,:E«.,rpy] j
DRY MOLECULAR WEIGHT DETERMINATION BY
SMPLIN3 TIKE (24-hi CLOCK)
NET mg Kl og SAKPLim LOCATION
FILTER NUMBER 3 TOTAL BACK r,g
FIKAL mg lrmit. „....„: ,t..,. .,.,p.sr.
S4I.-P1 F TYPF ;R*r,, INTEflRATFD, CONTINUOUS*
ASA! YTICAL KETH03
s> .-;<. i~'* i": t " v; ^; t1 i!':*^" :'-
1ARE tng »;;:'.:«:• a::- civr.-. :_•:.. ;SE: t<
NET mg f.r,l,i__,™T-.-.^,^,-,,=,^T
CYCLONE iwSJ'^s-'el"^ :);=?!•:"!;"'
FINAL m '* "»=i«s;L
TARE mg slwa - K1L
HET TtlQ ^J^y;--»-"-r-v...",-r-.-^-^"c:^-*c
TOTAL FRONT _lliL "9 *^%;V!^:f;£:" '^L«v--'p"
WMIfWi^E.
jw . SK»*itt D(T!
•f\ J i SCOTT INVJRONMEN1*,! TICHNOlOG^, INC
"^^ R'JN i 1 | i I [ ,VEFWE !
Wj"""^^ '« JS - S^ » *S;
C£7 1 ^ ^ ^
F.i.w.'^rtS'jiACRjM, iOi~ rl^1^ I *-
i*- t I i
CO. "IT 15 «CTi*l C&
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-------
PROJECT NUMBER ^ 7e s TEST NUMBER
-159-
FIELD DATA SHEET
f] $COTT INVI
PLANT
tion'X CitA-f'OV //i-^i^y^C-in /3.C.4 PR
QBE L£
DATE f 2,/?pf J NOZZLE I
NGTH S
.0.
TYPE fei^T ojy
.^^i- '•'
SAMPLING LOCATIOH ^ictCT iWu ioi^J-ffj-f SAMPLE BOX NUH3ER $ AC Xv
SAMPLE TYPE
FYRITE ANALYSIS
co2 o2 —
.T~ { J HETER 80X NUMBER i7 f1 ^ 32- .
RUN NU1BER "i'' £* PROBE HEATER SETTING , r/i r=3>
OPERATORS 3- L/y F!
LTES HEATER
AMBIENT TEMPERATURE *• <"" REFERENCE iP
BAROMETER
MSlI
IWCCBt
* !
:
„
t
T
V
fl <
1,
3
tSAVtSSE
Miir
SUWER
SETTING '• 't1
37
•-, 2^ READ AND RECORD AIL DATA EVERV 'S7 MINUTES
a
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COHHEOTS
iraV*.^l.rcf/^0' ^'~'^ /"'^
VMIKJX.
is, Hj
ISPCTCf
IEWIR5T
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"COHMENTS
'
-------
JOISTURE
FINAL VOIK'E .
INITIAL VOLUKE,
HET VGLtKr'E .
-160-
IILICA ca
FINAL WEI3HT l_Ll^± t
INITIAL HEffflT .£/• : , „ • ! /
NETWEIOKT __TL.±.|'
HOMOGRAPH DATA BY
_,. ml
__»!
__;>,! TOTAL ra$TUK£
ANALYTICAL DATA BY
ACETONE FRONT WASH ACETONE BACK WASH
FINAL '•' ' - -" ,- Big FINAL ff;<3
' — f "
TARE •'/ ' ' " •' / mg TARE Fig
NET " - - ~r mg NET mg
FILTER NUMBER 1 ETHER-CHLOROFORM EXTRACT
FINAL . '•'''•' '( ng FINAL mg
TARE "*~,yilf) mg TARE mg
NET .,V'/.C' 7 mg NET 133
FILTER NTOER 2 WATER. EVAPORATION
FINAL mg FWL mg
TARE mg TARE , nig
NET mg NET rt,g
'
FINAL Pig , rs,,-r, -... -., .;„ ;• r-r,.f[
TARE B>5 *;;-,.^"-,,"r .;:/in*':"" ..•'^H'i-'er''
NET mg *.-, -.-—»^^— .-.,-». ^-,. . „
FINAL mg »«" v^'si'.""'"
TARE mg SI- :- [!^—
NET mq *:t? -"'•.'r-^-^-rr-f.r-. --J'\;.i-rr,
TOTAL PROMT 151^ mg A:-;. «-t:- -^i.::..:. I.:':-.-..-::. '
COTt IHVIBONMtNfAL IECHNOIOOK, INC.
F( ^
»»tR«t5UC>.-tr>-.-FSTUPE 'i 1 /
PiUlM" VCLCCiTi- Hi AD. !«. H,(! «fcjli
CFJCTW | ^S
ciiaiLf ;c: !,~:j,t PHVETEF. ». j
t^«i.!.:i:.Lrii"-:iss... , J i1 1-
"* ! ' '^" 5 i
DRY MOLECULAR WEIGHT DETERMINATION BY
SAVfLIM TIVE {24-ta CLOC-Ki
SA.VPLI!(5 LOCATION..... .. ..
Sft'.'PLf TYPE if AC. 1S1EGRSTFD. COKTGiUO'J3)
ANALYTICAL KtlKOD
A.V8IFKTTEYPERATURE
r"*v. Ft -*i j 1 J 1 J 1
"~^^ ' H'KlL ("It* J ' »'"-•»' K£f
t« --^. F<>:I« S'T i K<:.« *•' I »:S:A-. "-1 ""'•I''1-
" " ! I '
st ;.:*.•-, *' v/; *CIu^ 1 o •« -1-
j ^S j_ h_ !/-, &
|-~ UJ t-j
18;
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1
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-------
#2705-01-0380 -161-
APPENDIX C
PARTICLE SIZE FIELD DATA SHEETS
i Scott Environmental Technology Inc.
-------
-162-
Date:
Operator:
AMDERSEN STACK SAMPLER DATA
Test /Run Number:
D
From f ••§
Meter Box No. _ g ^ (.
8r/dscf
&AHa t . 7£ Andersen No.
Nozzle Size , A ?
Est. Sampling Time 4_0 c c t .
1) ryt s t ;, i ' ,-, ,. e 0 ,/ t
Sgmglifig_Locatign & Point Number: Outlet AjnJSB| Point
Average Velocity Head
From 12 Traverse, A?s
Flow Setting From Nomograph, &H
Starit
Time:
Average Stack Temp.
From -12 Traverse, Ts
Reference AP
ElapSjgd
,
In
min.
Out
Avg,
Gas Volume: Final fc.£,| (£4^ c^*
Initial6M . 35"8 cf.
Meter Temp: Final
Initial
Total f''- cf.
Stack Velocity Head, &PS ,11 Flow Rate, iH 1 ( 2 5"
it • T< ft/ /«\ '•>'"/ / r«-^ Tl^««-f »- T?~^-«_ «1 M,
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (mg) %
l J3^3 2>^&* ra-<* «<**4is-.4r
2 ,11^4^ , ZgtfS" '^6' (
3 J3G7 -241 1 1 i°-^
4 Jzt,t^ . 15-4 8 28-^T
5 J35T- ,(/|6^ 13, £-
6 IZS-^T ,12-74 t-S^"
7 .f35-«- .^3fo3 X
8 IZ4Q& -IZ5I -2^"
Stack Temp, Tq 2.'"f7
It/
BCD
Cum. % (Microns)
• Back-Up __
filter ,2011
-------
-163-
ANDERSEN STACK SAMPLER DATA
Date: )?. . 6-71
Test/Run Number:
ty
Operator:
^x W4
Brain Leading From *ii
Meter Box No.
gr/
SAHa _ Andersen No. <5cf *V
Nozzle Size
dscf
Est. Sampling Time
min.
Sampling Location & Point Number: Outlet/Inlet; Point
Average Velocity Head
From 12 Traverse, APS
Flow Setting From Nomograph, iH
Start
Time:
Average Stack Temp.
From .12 Traverse, Ts
Reference AP
Stot
Elapsed
In
jain.
Out Ave.
Gas Volume: Final
8
cf.
Meter Temp: Final
Initial
Total
Stack Velocity Head,
cf.
'
Flow Rate, AH
Stack Temp, Ts ffi.7.
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (mg) % Cum. %
l ji£?r -V743 ,,33,^47:ry8^r-
2 tlZ394 ,2443 ^p '
4 ,13 IT j5\3 Si. ^
5 .I'StA .K)C3 7-°'^
6t ~% Jt* /—\ \ X I / fi?
i f 3 *""^ i % *** * ' * '
/ /J
7 (341 J30| ''^
8 .^4^ ,\11°1 ^,°
•Back-tip -3 -,,-?! ^» ^
filter ,^°7^ -^M J
Ib-mole
dscf /min
BCD
(Microns)
SCOTT ENVIRONMENTS ', TECHNOLOGY. INC.
-------
-164-
Date;
ANDERSEN STACK SAMPLER DATA
Test /Run Number:
Operatori
Meter Box Ho.
gr/
Andersen No, _S_ej- 4?
Nozzle Size
dscf
Est. Sampling time
f ' ~T '"• e* 4-- f ™
rnin.
Sampling Location & Point Number: Outlet/Inlet; Point 7 )
Average Velocity Head
From H2 Traverse, APe
Flow Setting From Nomograph, AH
Start
Time:
Average Stack Temp.
From -12 Traverse, Ts
Reference AP
Stop
Elapsed
rain.
Out
Avg,
Gas Volume: Final 4
Initial It,
Meter Temp; Final
Initial
Total
Stack Velocity Head, &PS
Flow Rate, AH Z.
Stack Temp, Ts
*.?_ j _ f ,. _ -ftr. „ _ „ try, „ i^'A
CoiTfcC tfid Volunte
Temperature Correction
Taken From Andersen
Plate Tare (g)
1 J3LO
2 ,| "Z.-^^-S"
3 -^^^
4 J1S"9^"
5 J3C.45*
6 1 7 *r^i
7 .13405"
8 J^Z
-Back-Up o/nCL?
Filter ••&£>&(-
"7 "1 f rn-i-p H\M
^— / * {*->l ^TO 'W"*""X/fe, irt/"JH t-^ P i WH1"T""1I i^ I L^i
dscf 6egrGe-feo
-------
Date;
\TL
-165-
ANDERSEN STACK SAMPLER BATA
Test/Run Number:
A
Operator:
Meter Box No. 5 ^ IV G &AHa /.g? Andersen No.
Nozzle Size . 37$"^
dscf Est. Sampling Time min.
gr/
C e 6 <
* ^r^.. ^^%
Sampling_J.ociation & Point Number: Outlet/anlej^ Point 2-P
Average Velocity Head
From f2 Traverse, APS
Flow Setting From Nomograph, AH |, 6L
jitart Stop_
f ime:
Average Stack Tecip.
From >H2 Traverse, Ts
Reference AP
Elapsed
In
_min»—•
Out
Ave.
Gas Volume: Final %Z,B"]1 cf.
Initial % 1. ^ cf.
Total * r3® cf.
Stack Velocity Head, APS . \ [c
MoiatutC" -From-i4 (%•) 7_r? , 1
'Voi-uree
Meter Temp: Final
Initial 4 \
Flow Rate, AH \ &1-
\
Coo-Deaeirt-^
Stack Temp, Ts
'* Ib-mole
dscf
Cor r<>e feed
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
-5
6
7
8
Back-Up
Filter
Tare (g)
Final (g)
Net (mg)
Cum.
BCD
(Microns)
• 4
.0091
iwr
-------
•166-
ANDERSEN STACK SAMPLER DATA
Date:
Operator:
Meter Box No.
Test/Run Humbert S~ D^
&AHa
JUcV 5,,.;
J.'XOt3 « "-J1
gr/dscf
Andersen No.
Nozzle Size
Est. Sampling Time
min.
Sampling Location & Point Number: Outlet/Inlet} Point _2O
Average Velocity Head
From H2 Traverse, APS
Flow Setting From Nomograph, AH
Start
Time;
Average Stack Temp.
From .12 Traverse, Ts
Reference AP »
Stop
Elaosed
b ,
In
0tit
Avg.
Gas Volume: Final st9!l'
Initial ^gl. Z-O^cf.
Meter Temp: Final
Initial
Total " '^S**cf.
Stack Velocity Head, APB , \(t Flow Rate, AH L .8 V
»» « -n IT/ /=, \ /^ « n „«<*- 1?^^ ft-j »/.
OrtclrCeil vCriUtmJ US»Ci; <>wt"tUCl.liU""rJ.v»»~iwjMi>»
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (|) Final (g) Net (mg) %
, i 5' 7, / N
1 Mff ,ixi« 4,3(iU.3)
2 ,U<-r ,\108 2'^
3 \3Col J374r '7^"
4 [254 .UTS
5 '3
e ,izsi -iirg. 'r
"* UK •—- 1 ^K ' |
8 ,a5l .l258tT l|r
• Back-Up •>-«-. ^x~.o^ o
Filter -2^ai -2084 ll
2,^4
Stack Temp, Tft ..^P^— '
' Ib-mole
dscf /rain
ECD
Cum. % (Microns)
,
srnrr
tFrHwntor.Y. INC.
-------
Date: tZ •£» -7*?
-167-
ANDERSIIN STACK SAMPLER DATA
Test/Run Number:
Operator: W tsL ... p^
Grain Loading Frocr f— y
.
Sampling Location & Point Number: Outlet/Inlet; Point
Meter Box No. ic.o44~ ft &AHa / , g? Andersen No. -5c4-
Nozzle Size ,
dscf
Est. Sampling Time __ | S" J<_C. , mln.
Average Velocity Head
From 12 Traverse, £?
Flerw Setting From Nomograph, AH \ , 8 ?
Start " Stop
Time:
Average Stack Temp.
From .\2 Traverse, Tj
Reference AP
374
Elapsed
In
Gas Volume: Final
Initialtfjj?\.
Meter Temp: Final
Initial
Out
*° 4l
Total "' '" cf.
Stack Velocity Head, APS T .'I 4r
111 ^
Moia'tuge- "Frot
Flow Rate, AH
Coe-Dongjrfey
Stack Temp, Ts
JiL
lb-mole
dscf
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate
1
2
3
4
§
6
7
8
Tare (g)
,1384
Final (g)
.1421
I3H
.[189
, \lftfc
J
.unr
Net
-------
Date;
12. - 3
-168-
ANDERSEN STACK SAMPLER DATA
Test/Run Number:
/T. 7 0 5"
Operator:
39,17
'Loading "Proi
Meter Box No.
gr/
Andersen Ho. TJ
Nozzle Size ,37-T
dscf
Est. Sampling Time
min.
Sajjnp.ling Location & Point Number: Outlet/Inlet; Point 1 1.
Average Velocity Head
From 12 Traverse, £PS
Flow Setting From Nomograph, AH
Start
Time:
Average Stack Temp.
From H2 Traverse, Ts
Reference AP
Stop
Elapsed
iO 5ft, min.
In
Out
Ave.
Gas Volume: Final \-^_o Q «n cf.
Initial Rl. S"8R cf.
Total
Stack Velocity Head, APS /t^j
Mister Temp: Final
Initial
Flow Rate, AH 1 . "3 ;T
Stack Teisp, Ts
27
, j-njl-ja- TI-
vtOl. i wwt-cfO- VOitlUHd Qod fcFv"4,T"3?T- v t.1 Cud i i.O"W""!ci&S>**"
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (ing) % Cum. %
1 .13*18 .ZI2J ni*H3*3«*0*
2 ,00^ ,1108 40.^
3 ,i4osf j^cjg za.^
4 .infc ,u^r (fca^
3 .13-15- J4SS ^3
6 JZGsT .t2^Z5' M?
7 J^o .mi ^
8 ,/Z^C, l^oo *A
lb/lb-mole
dscf /min
BCD
(Microns)
•Back-Op .2.O73
Filter
PKfVIBrtMMFWf Al TfrMNfllOGY. INC.
-------
-169-
AHDERSEN STACK SAMPLER DATA
Date:
11 * g . 7^
Operator:
Test/Rua
Meter Box No. &&Ha
TIAJTI Tnju-HriP Frrr.'u H ri
7 J. Eat J-** iJv£3,\J JLil^ i. Jp. Wii* if ™#
gr/
Andersen No. S&T Z-
Hozzle Size
dsef
Est. Sampling Time
, : I c t M a-"i t,
Sampling Location & Point Number: Out let/ Inlet; Point -7.
Average Velocity Head
From fl2 traverse, &P
Flow Setting From Nomograph, AH
Start:
Time:
Average Stack Temp,
From .U2 Traverse, Ts
Reference AP
Stop
Elapsed
In
min.
Out
Ave,
Gas Volume: Final
Initial
Meter Temp: Final
Initial
Total
Stack Velocity Head,
Flow Rate, AH
Stack Temp, Ts 3
Hoiaturc -From-ffA (%•) 7 "* 2'- Coo Dcnoity- P-rom- i3 Mj
BOTT eeted • VcHhme dscf Ceg-ccetod' Flow Rofca-
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (mg) Z Cum. %
1 .OfeOJT ,24lfe l3s.ff^-^-2ob^
2 ,i2ro j^ol <*r,i
3 ,!3to J^e^ ' 32,^
4 , ia.5"Si" . [43^ 16.05-
5 , i35r^r , i4'(-> r' ic.qr
6 , 1300 ( \3~3S" 3.T
7 .i^^r ' ,,st, .)$•
8 ,UTi >l2yfe5- r6r
-Back-Up 2-Ol \ ,20lBS" •""• ^~
filter ' • 4
Ib-mole
dscf /rain
BCD
(Microns)
-------
-170-
ANDERSEN STACK SAMPLER DATA
Date:
80 s"
Test/Run Number:***"&,
Operator:
Grain
Keter Box No.
gr/
dscf
_ &AHa Andersen No. 5 ef~ 3
Nozzle Size
Est. Sampling Time jj-JF
min.
Sampling Location & Point Number: Outlet/Inlet; Point
Average Velocity Head
From 12 Traverse, APS
Flow Setting From Nomograph, AH
Start
lime:
Average Stack Temp.
from -12 Traverse, Ts
Reference AP
, 2, i
_Stg£
Elapsed
In
jflin.
Out
Ave.
Gas Volume: Final 17/5' g $T\cf.
Initial }1fy 4 I \ cf.
Meter Temp: Final
Initial
Total
Stack Velocity Head, AP
„ . ^ .__ T, „/. ,9\
Gon-e-ted V-"ufce
Temperature Correction
Taken From Andersen
Plate Tare (g)
1 ,!3$*t
2 J2.U
3 .i3(p«r
4 .1Z54S"
5 .131(7
6 , \ 2. tG'^
7 .131)
8 ) Z415"
'' -H.J O df> "f
< IvJL *
s . l^ Flow Rate, AH 2 .IT"
-*- /-^"" • < «>s ^
n r* f* 4" f^flT" l*Off^ t"-f^"O ini r 1 OVJ»nHru.iLi t £W
Factor for Aerodynamic Size of Particles
Manual, Figure 3
Final (g) Net (mg) %
? lC5 ~7^.4-i-Ub,0$";s rtU,2^S'
I *«• t J ••'
,H"54 ^""''^
. l(/78 ' 3>l.3
,1512 ze/r
.15*2.^} 15.4
.I35fc fe-^
.I37C, -^
^2.4*1 5T -*^
Stack Temp, TK '^^'tf
T l)"*iQo2.e
dscf /min
BCD
Cum. % (Microns)
•
Filter
-------
ANDERSEN STACK SAMPLES. DATA
Bate:
Operator:
h ,-:,
iTlS^ " i1TOID. 1! ^
Meter Box No,
gr/
Test/Run Number: 110
&AHa
f / A
Son H
Andersen No. 5e4
Nozzle Size , "3 7
dscf
Est, Sampling Time __ 3>Ts<-'C. min.
^,
Sampling Location & Point Number: Outlet/^tnleJ); Point v 7
Average Velocity Head
From 12 Traverse, AP
Flow Setting From Nomograph, AH
Start
Time:
Average Stack Terap.
From-12 Traverse, Ts
Reference AP
Stot
Elapsed
In
Out
Ave.
Gas Volume: Final feH 0 , t)°Pcf.
Initial
Total vcf
Stack Velocity Head, APS . 1 5""
Meter Temp: Final
Initial
Flow Rate, AH ^, 1
Stack Temp, Ts
V • ("n -,;-,,- f TV, -I* T- .0 M
ep%y-i*l* i- *--.«_jJ-»- 3Il,-»t-'l-T ...T.I...-X f* f* f* -C £^"fclfMilU3kf* f~ ip'ijri i Hi /"*•* * 15 **t *- j-i
wJ. ^. Cr Vw C. t-Ul M ITT i r^irt^ Vi 2s v- JL ymH1l'T'- f"l=r,^v-"*p'«it -F 1 V^fr '" **JL¥-%-%*1'1
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (mg) % Cum. Z
i j/ih'*) "*. n 1 m i *- s"k,^r£34
. ( 'i U ''-J o i / 1 ' ' ' • '
2 .t lc' -1 1 33*1 k1^
3 ,140° .neb • ^.t
4 ,1231 J3"?S 14,1
5 ,13 A3 : ; J4o3 _ 6.0
6 JIB0* • \3c?4 | ,5"
7 ,\406- J412 ,4
8 , 1 2- q ^ . 1 3O4" . r
-Back-Up , ' a
Filter .i-O^Z. ,?-ObO
•44 J
"'ih-mole
dscf /min
ECB
(Microns)
1J V C I *j">«>Sw> «>k
-------
Date:
2.-7.
Operator:
..
bar "- •
Brain1 Loading From
-172-
ANDERSEN STACK SAMPLER DATA
;**_,
Test/Run Number: _27OS'/D Dd I
Keter Box No. &AHa_
gr/
Andersen No.
Nozzle Size
dscf
1st. Sampling Time
min.
Sampling Location & Point Number: Outlet/^
Average Velocity Head
From H2 Traverse, APS
jSo^-K
Point "7"/
Flow Setting From Nomograph, AH
Start
Time :
Average Stack Temp,
From -H2 Traverse, Ts
Reference AP
_Stog_
Elapsed
In
Gas ?olume; Final
Initial (..-:
Meter Temp: Final
Initial ($
Out
Avg.
Total
Stack Velocity Head, APS
Flow late, AH 1 1,
Stack Temp, Ts
Moisture— From fl4 (•%•} / ••>. '; Cao-Panal'tv^ftFea fl3» fi4
e
-------
-173-
ANDERSEN STACK SAMPLER DATA
Date: //?.?• 7f
Operator:
" -•2 — T'_- J J_ ,, r, TJ-i-j-nn *• r
WTSXTl UQ3CI-oi£ irtuiu ll'TJT
Test/Run Number:
Meter Box No. &iHa
/*
Z70r/& V^t 50^-1*
i
aS*
Andersen No, :5<£r • jf
Nozzle Size
° dscf 1st. Sampling Time min.
Sanrpl ing Location & Point Number: Outlet/Inlet^ Point
Average Velocity Head
From 12 Traverse,
Average Stack Temp,
From -U2 Traverse, Ts
etting From Nomograph, &H
Start
Reference AP illrf
Stop Elapsed
30 ^e.
^
min.
In Out A
Time:
Gas Volume: Final ^f I
Initial ^
Total
Stack Velocity Head,
Meter Temp: Final
Initial
Flow Rate, AH S. "*-•-
0
~
31
5T-7
Stack Temp, Ts
»» . x. „. T> _ «r/ /<'/^ -• •- <•" /•• -n^ 4«-,. !?«.„„ «-5 M,
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Plate Tare (g) Final (g) Net (mg) % Cum. %
1 4^1 ,E7l4 B\,~R rJM>";- a'i'i^r
2 .I25"i? Jv?^ ^.°l
3 j4"S5" .1112^ - "25.1
4 .^S6 .ri-.^t iA.l
5 .13S^ ,; /:.''" 4,9
6 .IZ6Z ,]2P'- US'
7 .14($~ U« ';3 ,4
8 ,lH7 U7;p a
-Back-Up 7 . -,,- , ri r, a
Filter • •'- '^ t^ • - v " '-•! . ' *
lfc/lb-tQole
dscf /min
BCD
(Microns)
-------
-174-
,. ANDERSEN STACK SAMPLER DATA
Date; /J' - _>".'. ~>_ 9 __ Test/Run Number:
Operator; <> •__..!. Meter Box No. ^-^XlL,, - &i^Ha !' ''-">•' Andersen No. -g.^ J^
Nozzle Size „ 2.5'.'*'
gr/
grProa "f -§ _ 6 dscf Est. Sampling Time f r ,: ,.•,..,..„ mln.
t * j '
Samplingml»p.c.ation & Point Number: Outlet/Irlet; Point C '. if".••''<•--'.'«L— -^i.,-^-<..' *— 3 *•* f\
Average Velocity "Head ...•- ,-/ - • ' Average Stack Temp,
From 12 Traverse, APS ____i___ From -12 Traverse, Ts
Flow Setting From Homograph, AH -o »/ Reference AP ? ? ">
Start Stop. Elapsed
Time: ' <^ :v:'«v ,-j< -J.x"vV.c min.
In Out Avs?.
Gas Volume: Final ?^Tz£*$%fcf. Meter Temp: Final 7^' 7,"2-
Initial ^7-^5". Vf-Xcf. Initial 7 2 72
Total
Stack Velocity Head, APS Flow Rate, AH 3 , 1 Stack Temp, Ts "'''
®~4-3. MH Ib-mole
•tecHVoitnsie dscf fei?*«et«d—F-lew-tefea- dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3 _________________
/TtVu/t Usr\\f-t ' J -y
1CD
Plate Tare (g) Final (g) Net (mg) ' -r-'-Xr "" Cum.' % (Microns)
1 .1390 ,\(,ZS w+M^zbW
2 |Z4"7 \S"^3^ 34.u'
3
4
5 ,|37
6
7 ,|2>S"& t ISB'lf s-^
8
-Eack-Up
Filter
-------
-175-
ANDERSEN STACK SAMPLER DATA
f,?,' ''
,J »-' \.,* x". •
Date:
Test/Run Number: fj .~
Operator:
Meter Box No.
&&Ha ;'', ^:'! ' Andersen No. '''•*: .£>
P 1 °\
-------
Date;
-176-
ANBERSEN STACK SAMPLER DATA
Test/Run Number:
Operator; }'< ) (: "-
From"
Meter Box No.
gr/
&AHa /,"'*)'.- Andersen No.
Nozzle Size
dscf
Sampling _Lo_cation & Point Number: Outlet/Inlet; Point
Est. Sampling Time _ / T"*:•.*-_
mm.
Average Velocity Head
From fl2 Traverse,
Average Stack Temp. ^
From .52 Traverse, Ts '-f'"' /?(')
letting From Nomograph, AH
Start
3'. I
St.0!.
Reference AP / *7 "3
Elapsed
*— )S~
In
tain.
Out A
Time:
Gas Volume: Final 9"? ^,
Initial ^7^, "2j%ct.
Meter Temp: Final
Initial
Total
Stack Velocity Head, AP
JrMri'G LtllirC- JF \. Om il "f \,* /
erft-*rr-« OT^-OI A —Wf*l i *«-a
Temperature Correction
Taken From Andersen
Plate Tare (g)
1 44D(
2 \ 4*4* L>
3 .) 3^^
A \ "\ & ^5
5 ,132.^
6 .IZ8Z
7 f*j41
R
.Back-Up pO44
Filter
, 24 &Cf .
s Flow Rate, AH Stack Temp,
7 #"""'"' J
I ^ ^^C*tJ T_r*etf tJX i.y t I.tJi.lip s1^ ^X
Factor for Aerodynamic Size of Particles
Manual, Figure 3 ,
f™*" 's *» t i \^f" i / ***• "1> t*i
/ i'O" ^ *f I VtiP *1** 1 *****
Final (g) Net (rng) —I'' Cum. %
,2 ^ Ul ,5, 3C,i S?77,77V| ^ ^ y,^^
,x442 \zr.o
,2U7 7^.1
,116,3 47 J
,H?18f 3S,5"Jf
,(4^^ 24,4
-iAli |?.4
,lV7 3.1
n
Ts
•b'lb-mole
dscf /min
ECD
(Microns)
•^rr^ .:'.
-------
-177-
ANDERSEH STACK SAMPLER DATA
Date;
Test/Run Number: _ /
Operator;
6)?flit5" Loading Prora
Meter Box No.
gr/
Andersen No. f
dscf
Nozzle Size
Est, Sampling Time •'• -
min.
• . f • ,', •- • .,'•' '
Sampling Location & Point Number: Outlet/Inlet; Point ._••_•_'.'s. ;" ••. • _.. .> ,• ..{.''{; .-.'' "',- ••*:y^*r:-
Average Velocity Head
From U2 Traverse, APS
/
Average Stack Temp.
From J2 Traverse, Ts I(• (:*
Flow Setting From Nomograph, AH hi
Start '
Time: ' C?
Reference AP' * -'
Elapsed
/..',-,.at.:j,<.
Gas Volume: Final tf 1-*J % £ Z.zf •
Initial tf?3, ('/••?.' cf.
Total , 11 ^cf.
Stack Velocity Head, APS
In
Meter Temps Final /Q '/
Initial //
tain.
Out
Avg.
10 0
7.4
Flow Rate, AH
anolt-v—F-
Stack Temp, Ts
u/
Ib-tnole
6orre e ted~ Vcrlmae
dscf
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3
Flate
1
2
3
4
5
6
7
8
Back-Up
Filter
Tare (g) Final (g)
403
Net (mg) '"^4-
83.-;= =13.0 7r,56ST <3S-,*/W£
14,0
, o
BCD
(Microns)
t- -^ -j
iD " ** /
2
,130-5
,2,0 6 ",
SCOTT ENVIRONMENTS I TECHNOLOGY, INC.
-------
-178-
ANDERSEN STACK SAMPLER DATA
Date: 17.-^ ~")^_ ___ Test/Run Number:
Operator: /. ''•' ' Meter Box No. _S^_ SAHa Andersen No. / |
2^O^ Nozzle Size /•'-''
8r/
6reia fcoadiTtg-Pron• f ••••S' _____ r r 6 dscf Est. Sampling Time •'-'•..'- • ,..• min.
f. *^^mvmmm """""' , ' '' "' ~m"' ™ ""
(• ^ / i • '•
S^pliSS_L££Jl£i2a & Point Number: Outlet/Inlet; Point ^h_:_> ••_ [•' > .n:lf"t" *'"""''-'•' "%'>--'"*"v-
Average Velocity Head • , -. Average Stack
From U2 Traverse, APS . !/& _ From \1 Traverse, Ts
Flow Setting From Nomograph, AH ^" ' ^ Reference AP
• ^ G
Start Stop Elapsed
Time: ' & /o ^c-<, • / ^** min.
In Out Ave.
Gas Volume: Final <^52S3|ti5§2.cf. % 30, fla^Meter Temp: Final / (jQ
j~ *~* _•- / C-
Initial''*^,^S£&cf. Cj%A 73 ?„ Initial /1
3 ,138
4
5
6 \Zb5 43 ^^ 10,2
7
8 .\ZV7 ,\15"6 ^-!-
•Back-Up .2.OTO . 2. U I' 4'\
filter
I* V 1 1 trrtrr Ci.i\/n>««juck.i
iTAi TC/-ufcjr«i nriv
-------
Dates
Operator:
-179-
ANDERSEN STACK SAMPLER DATA
Test/Run Number:
Meter Box No. ••" SAHa
Andersen No. ••'
•fcoadittg- From -f -rJr
gr/
Nozzle Size -
dscf
Est. Sampling Time
min.
& Point Number: Outlet/Inlet; Point
Average Velocity Head
From f2 Traverse, AP<
Flow Setting From Nomograph, AH
Start
Time 5 ' ^
Average Stack Temp.
From .?2 Traverse, Ts
Reference AP
*r— /
, .S t.
Stop
Elapsed
In
min.
Out
Av».
Gas Volume: Final C'ji /
Initial ciZ$t7:^'
Meter Temp: Final
Initial / B&
Total
Stack Velocity Head,
Flow Rate, AH
Stack Temp, Ts JT77___
Ib-mole
d»rrecte d- ¥oltnae
dscf
dscf/min
Temperature Correction Factor for Aerodynamic Size of Particles
Taken From Andersen Manual, Figure 3 f, ^
;c>. ^/-'u,'/ " V
Plate
1
2
3
4
5
6
7
8
•Back-Up
Filter
Tare (g) Final (g)
Net (mg)
Cum.%
BCD
(Microns)
.3ST
z.i
3,3
,1414
-------
12705-01-0380 _180_
APPENDIX D
VISIBLE EMISSIONS FIELD DATA SHEETS
Scott Environmental Technobsy Inc.
-------
•/C^^AsJd
Distance to Stack
Wind Direction
Sky Description
PLUME OBSEKVATION DATA
Run No.
Plant (J,
Location
Observer
/ Date i.'
-VL/^-1 L-/MX^-/(C
rlcft /}^2-^
-^ ^ li/i „
J 0^ / " /A
Time Begin J D 1 S
\ f- {
Stack Height X ^
^/ 7 / / 1 Proj ,1
/ /
^
/? P
^\^. C\^JL
-VM-v-f!
End i X-3
/ f] 0 '
Speed
Sum of Readings
iTgtal No. of Readings
CX3.
1
Opacity = Sum'of Readings
Nc. of Readings
Environmental Technology
-------
0
VW*
X1
o
*— j.
i
3
3
•—»
R»
W»
A
zr
g.
r9
00
v:
X
t »
Sec
Min
0
1
2
3
4
5
6
7
, 8
9
10
11
12
13
14
JL5,
16
17
13
19
20
21
22
23
24
25
26
27
28
29
0
0
TV
u
D
0
0
'
-^
D
0
o
7)
0
0
o
0
..,
t,--
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/I
D
D
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D
0
0
0
0
J>
L -•
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D
15
0
D
D
O
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o
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&
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30
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o
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45
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,_
0
c>
i-"'
i
.'•' -'
U
c>
O
>
o
c>
'---'
.-A
v>
Sec
M-fn
i
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
| 47
48
1 49
1 50
i
C 1
in--- :
52 |
53
54 i
55
56
57
58
59
°
_
u
0
3
..'^
-T)
&
•o
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'-*
.'-.
f'\
0
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V.--
"
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d
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!
t)
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/-j
0
f:;)
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— i
15
O
-"••*,
-.3
;_J
'•-•-
:,?
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O
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rs
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/**
0
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0
30
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^
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0
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0
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45
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0
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^
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0
0
c>.
'0
P-N
'""' ]
•-..:• \
0 |
'• —I
C t
- J - HT 1
«D
PLUME OBSERVATION DATA
••> -•
Run No, ' Date • -- • •* < •• Proj.ff
Plant ' !••'.-.-:•••. • .'• r. '.-."•.
Location ^r:--~f ;/.••••'"••"'- j -/ i' Speed 0 ' "' f'f ''
Sky Description L-^-' j"--"1^
i
Sum of Readings ^
f\3
1
Total No. of Readings
rt^^^j^,, _ Sum of Readings
No. of Readings
_
rTf^^. i c--c^/^7x/^r^n"-''^
J"*'^ 'A '^-3 "'""^"^ J ' '' 'i ': '•- 1 1 i
*" ' V, • \ - r *.'" - • '{•• V .' "-, , \ / .•• "^ > t' ' f r ', ^ ** "
<-~ ~ £ '•*,; ''--•/ -/i"" -4 "v,-" *_-*'" i*i-**i^f ^^t-j^*"^ 1«*i~ 'Sjilk'
*. •:£V"i?'- -1
5",—,..* L-,*wa Envifonrncntn! f ochnology
-------
Sec
Min
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18 '
19
20
21
22
23
24
25
26
27
28
29
0
5
D
O
o
o
O
o
o
b
0
D
D
0
D
D
0
0
U
0
x»
0
0
D
D
0
0
D
O
\)
,• >
15
*
0
o
O
o
3
ts
0
D
O
O
5
O
O
»p
0
D
O
O
D
O
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o
p
o
0
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D
6
0
o
30
0
o
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0
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D
P
O
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p
Sec
Min
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
0
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t?
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• '•.
. '•** J
PLUME OBSERVATION DATA
Run No. >•
Plant U A/vxJtx-
Date
Proj .]
Location ~ufu ft/
f
Observer
Time Begin^ _\
Stack Height
End
! \ } o
Distance to Stack
Wind Direction
Sky Description
Sum of Readings
Total No. of Readings
Opacity = -
No, of Readings
CO-
CO
I
vr-N/
a 1 **-f?.*?~ -j
fe_ai±:^J
H FT
' '
Environmental Technology
-------
o
•-*
*-t
rn
I
Sec
Min
0
1
2
3
4
5
6
?
8
9
10
11
12
13
14
15
16
17
18 '
19
20
21
22
23
24
25
26
27
28
29
0
!
—s
W
; •%
.-"""I
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0
0 J
i
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-';
I
'» ~
Sec
L Min
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
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OUTDOOR LOCATION
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FucrnvE EMISSION INSPECTION
OUTDOOR LOCATION
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FUGITIVfc EMISSION !MSiJECTiOM
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__ -217- _____
FUGITIVE EMISSION INSPECTION
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Wind Speed 'C1 —
Process Unit • (0/!& &*- ffi-T
"Sketch process unit, indicate observer position relative to source and sun; indicate potential emission points and/or
actual emission points.-^..ti •' ...•>. ... . r- (^(c^<. /m.,-? •'"•
OBSERVATIONS
Begin Observation
Clock
Time
6^,1^-
C'7:'16'0::'
/1,-tAJ'^A
fl.'
Observation
Period
Duration
(Win: Sec)
c-
Accumulated
Emission
Time
(Min: Sec)
' O
0
J//
o
O
Q
O
o'« o,
C,
o: y/,
o
JS;r<-
End Observation
-------
-218-
FUGITIVE EMISSION INSPECTION
OUTDOOR LOCATION
Company
Location
A
f
Company Rep.
• Sky Conditions
Precipitation
0
Inspector
Affiliation
Date
Wind Direction
Wind Speed
\( <-,.
Industry V ""^_
<*?<•£
Process Unit <
Skc-tch process unit, indicate observer position retative to source arid sun; indicate potential ejTiiislon poi'nis ar.oTc'r
actual emission points.
—1
L_
('
OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(Min: Sec)
AT
O
&
O
-'•cv-
-------
-219-
FUGITIVE EMISSION -INSPECTION
OUTDOOR LOCATION
Company
Location
/{• ]'__ .>--.-; •Q ...4.
Company Rep,
Sky Conditions
Precipitation
Industry
Inspector
Affiliation
Date
Wind Direction
Wind Speed
5'V
1 ~/G
Process Unit
"Sketch process unit, indicate observer position relative to source and sun; indicate potential emission points"ar.d7or'
actual emission points.
OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(Win: Sec)
'3c
A ~
Accumulated
Emission
Time
(Min: Sec}
_jQ
End Observation
-------
-220-
FUGITIVE EMISSION INSPECTION
OUTDOOR LOCATION
Company Ui-UorJ ^rt/*U?>j0i,
Location ;v--r Sft\/t\n?> /j-thc
— - ••- j .. . .
Company Reo,
Sky Conditions Cc^v
Precipitation °
Industry \J or-t ^.ot\is,^.
"inspector /7 ftlfn. <./&(-./
Affiliation S^OTT
Date /d/?/::/'l
* t
Wind Direction 6^, /u . 60^
Wind Speed •$"" Ajv^h
Process Unit -^^^ P/A'C',- -ir/ift-y/
Sketch process unit, indicate observer position relative to source and sun; indicate potential emission points ar.oV
actual emission points. "\v \
OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(Win; Sec)
Accumulated
Emission
Time
(Min: Sec)
o
o
-------
-221-
FUG1TIVE EMiSSIQM INSPECTION
OUTDOOR LOCATION
Company
Location
Company Rep,
Sky Conditions
Precipitation
Industry
Inspector
Affiliation
Date
Wind Direction
Wind Spaed
Process Unit
"Sketch"process unit, indicate observer position relativ^to source and sun; indicate potential emission"poTnts"ar,d/'c"
actual emission points.
OBSERVATIONS
Begin Observation
Clock
Time
Observation
Period
Duration
(Min: Sec)
jerec .'t
Accumulated
Time
(Mm: Sec)
-------
-222-
ffK-
INDOOR LOCATION
Company t J^V;
Location __//.'<
Corr.psny Rep.
inspcctor .
Affiliation
Date /P
Process Ur.it
Light iocctbn (overhead, bariind observar, etc.)
lilurr.irrjriC'.i (lux or footcarirfiesj *';
Sketch process unit, Inalcats obj.crver pointion relative; to source; indic^tr: potent^! ernisslo''. point? ?nd/or ccius
e,Til;sion poirui.
r" ' Fr 7""~Tr~~~~ T~" " "" ~
iv o o;, »"i v M i i v/1" i o
Clock
Tirr.s
Period
Duration
{Min: Sec)
J
ec
End Observation.
\ •
-------
>'H V -223-
~ ' T : \ ' 1 '"* * I •"" C ' ' • \ s ' '• i r- -> - »-N-T i ^ " •
« J41... Cn. I ,>N,U,, ,;%;-.: .:v, i i',,V"
Company
Company Rep.
Affiliation
industr
Process Unit
Light type (nuorescent, ir.cundcsccnt, naturs!)
Light location {overhead, behind observer, etc.)
inanso (lux or footcar.dies)
Sketch process unit, ir.dicotc obssrver positior, relative to source; indicate potential emission pc-Jnts und/or actua!
emission points.
OBSERVATIONS
Clock .
Time
Observation
Period
Duration
(Win: Sec)
Accurnui':tod
Emission
Time
{Min: Sec)
B-egin Oosorvation
, /v ; 1;>
End Observation.
-------
-224-
FUGiTiV,:
G\' IXSPSCTSGM
Company
Location _Jip"T
Company Rep,
Aff ilia tion
|2£li^±±-..-.
Process Uni
L« (, ^ f j; ~ » »^ »> w. -i. * ,~ f~ - r~ w ™ .- .- - t-, A - J. , , , I \
Jym iVpO i nuOi ;Ji*»t^' u, il i'.,cn.ji,.T'^t'< it, iiOtuiot,
Light location (overhead, behind observer, otc,)„_/?_!
illuminance (lux or [ootc3nd;e5)___^
Sketch process unit, indicate observer poiuion rc-'w';
emission points.
c-: ;o source-; indiccte poteniiai emission points ar,d/or s
/I
. 1 7'
X
Clock. .
Time
' Observation
P»-riod
Durotion
(Win: Sc^c)
Accumulate^
Emission
Time
(Win: Sec)
Obsc-rvstion
O
End Observation,
\J :a.o
O
-------
-225-
FUGITIVE ^r/,lSSiO\ INSPECTiOM
INDGGS LOCATION
Company
Location
Company Rep.
Inspector,.
Affiliation
Date
industry V
Process Unit
//*'<.(-,-
Light type (fiuorescsnt, incandescent, natursi) mj
Light location (overhead, behind observer, etc.)
Illuminance (lux or footcandles)
Sketch process unit, indicate observer position rehtive to source; indicate potential emission points and/or
emission points.
CESE.RVAT10NS
B-ecin Observation
Clock.
Time
Obser\'ation
Period
Duration
(Win: Sec}
Accumulated
Emission
Time
{Win: S&c)
End Observation,
-------
-226-
INDOOR LGCATiCS
Location \_W'
Co.T.pany Rep.
inspector_
Affiliation
Date
ci rr
1 nd u st ry_ Vi
Q
Process Unit
L
Light type (fiucr&scent, incandescent, na'vuro!^ i!l
Light iccstion (overhead, behind observer, etc,} ^Jii^JL
liiurnirKjnce (lux or footc^riciies}
Sketch process un^
emission points.
or>iorv2r position ro!tit;v.:j to soui'ca; inc'icste potential emission points end/or acius!
SStui VAT IONS
t >/><*.*. * wt'A--
Clock
Tirr-o
U T '-- "- *-Tr- -",
J^t:* v u uui J
Pcdod
Duration
(Win; Sec)
Accurnuiatad
Emission
Time
/!•.,-:„. c-,.\
V' II.! I. Oti'-/
B"eain Observation
C ,
0
Of ,'^t)
O
S-'/"'-*
¥•'••;
End
-------
FUGITIVE c,V,!SS;C,\: IXSPECT10X
INDOOR LOCATION
Company
Location
Company Hep,
Inspector
Affiliation
industry.
Process Unit
-./-
Light type (fluorescent, incandescent, natural)
Light location {overhead, behind observer, etc.)
Illuminance (iux or footcanciies}
Sketch process unit, indicate observer position relative to source; indicate potential emission points and/or actual
emission points.
OBSERVATIONS
Observation
Clock .
Time
' Observation
Period
Duration
(Win: Sec)
Accu mulcted
Emission
Time
(Win: Sec)
D
End Observation,
-------
-223-
FUGmVE EMISSION INSPECTION
OUTDOOR LOCATION
Company L/-1 , e /•, (\>/ A< c/<*. •
Location /A f *v :v, -\ c< «•; /4 r A: ^ ,q 5 r/ *5
^ J
Company Rep.
« Sky Conditions
Precipitation
Industry
Inspector ) f c^/.f A /x /-i-iAr/""
Affiliation Jco/t"
Date /^/f/79
Wind Direction
Wind Speed
Process Unit
'Sketch process unit, indicate obserx'er position relative to source and sun; indicate potential emission points and/or
actual emission points.
* OBSERVATIONS
Begin Observation
Ciock
Time
Observation
Period
Duration
{Min: Sec)
Accumulated
Emission
Time
(Min: Sec)
___o
G
End Observation
-------
#2705-01-0380 "229"
APPENDIX E
EQUIPMENT CALIBRATIONS
AND
SMOKE READER CERTIFICATIONS
Scott Environmental Technology Inc.
-------
S"F* it/"""
. xACr
rated by
•Tlcan Quick Connects
fr.errio-eters
Lights
rs t ,
' I •«.
Electrical Check - Aaphsn
Punp Oil __
Valves
<•> 1,'
Dry Test Heter.> r'
Buzzer
Leak Check at 27" ug.' - Leakage 0 k' ^ ^
Vacuum Gauge
I/
CFM
Date
- Han
Orifice
CF
CALIBRATION - ORIFICE AND METES
Box No,
:F . T.. IT .
Pb
0.5
1.0
2,0
4.0
6.0
8.n
.
/
~
.
P7
' .;
', ~j
\ *•
"T
Calculate Y 6 AH-g at r^a. 2.0
^. p, (^ avg. + 460)
CF. (P, -I- 0.147) (T,. 4- 460)
u D W
0.0634
Pb (OTd + 460)
/(T
4_lJL
-f 460)
T_oleranccs
CF
w
5
T"
: j. -7 P
10
V
AH « 1.6 - 1.84 - 2.1
-------
, Ca.'*•
ice
; ISO! , i,-X
0.0317 (Kan. orifice) /(T + 460) C \2 ' 1
f \f ^ 6
___ 1 k !! ynn !i AH
1 1 r ? ^
P. ^ ' i
0,1902 / ( m> +460) 16 \" I I I
- - - F,, - ' ? r n 3 / / S T O !
• • •• — • .'-•— -.'. -i j - J! 1(6.0 S l u ^ ^ l
±1 V^ (^0 +460)1 3. {f(lh I ! !
^™«»^ \ S t I «
. - ,-_„ ^^,.^^mI,W.._ -^ M^.. , ^
1 0.2536 . /( (T-& +460) \^\\ | j
j s iSsI
CF^ P (T avg. + 460)
Man. orifice
CF, (P, + 13.6 (T + 460)
do w
i
I 1 . fi^b y- ^/l > "^ o ( 1 tj ;'. ^- 460)
j - - _
1.031 (3,'[."if+ 0.0368) ( fc 0 + 460)
X/rSI x >,'7. x,)/i.'ir( /,-:T+ 460)
I . V V .f (V! . y r+ o . 294) ( /, ;^ + /»co)
I3.7VO x )/! V/> ( 1 r->? + 460)
4,1^1 (^1.^+0.441) ( .^'> +460)
ISV^^xM^
-------
-232-
Irh
o
o.
.:leaa Quick Corrects
#
Purap Oil
Valves /2.
Dry Test: Meter.
C r 3
Ltectrical Check - Annhenol
iariac '
Vacuua Gauge
Usak Check at 27" Hg, - Leakage
Isnarks
CFM
•ate
CALIBRATION - ORIFICE AND M2TER
Box Ko. ft C.
Man
Orifice
CF
w
CT
' Pli
0.5
1.0
2.0
4.0
6.0
8.0
f( ?
2 ' 7,
?,
-------
Date 2-f',T-l 7 *
0.0317 (Man. orifice) (T 4- 450) - "
V
CF Pt (T
Man. or_.L 1'
13.6
P, (OT, + 460)
b a.
(T + 460)
CFd (pb
-f 460) /O
6+ 0.147)
! 0.1268
0.1902
-------
-234-
STACK SAMPLER CAL13RATIOM SHEET
I
Calibrated by
Date ^1
Cleaa Quick Connects
Manometers '"> "C
Punp Oil
Valves
Dry Test Mete:
M
Thermometers
Lights
Buzzer
Electrical Check - Anphenol
*
Variac
Vacuum Gauge
Leak Check at 27" Hg." - Leakage _
Remarks
Date
CALIBRATION - ORIFICE AND METER
Box No.
• Kan
Orifice
\ 0.5
1.0
2.0
4.0
6.0
8.0
CF
w
) ^ "y- 9 ^
T. * -, " *:
7.^0?'o
*• ."* '
(•> .1 'S:
-' .-u-v;->
<*d
; r.-j. t
f ' • .'" -."• J
"/.li^
.-* / *"• '
^_ • V : '.'j
ccor?
T
W
"->
'-3
, ,-« '"<
~l
'-,^
•'"-->
"a
G^
/ O~^
_j^23
j^-:
\\Z
\\"\
c,_*
- ;. 7
s7 ^"^^
v •'."
V '.^
v>*)
Td
avg.
Jb
'• '» ,
C'\
on
/.-,-;,
..0
'Pb
^ C i ^* A/'
rO C •"<
^ V, ,.* /,'
,;:-. ,.•
l" * *"
*v. *- | i *
r / -_^ /
i^
5
5
10
-10--
-10'
•10
Calculate Y & AH/g at man. 2,0
Y =
Cf P^ (T. avg. + 460)
w D d
-5-0.147)
460)
0.0634
(T
w
460)
P, (OT, -f 460}
D d
Tolerance_s_
Y * 0,99 - 1.00 - 1.01
AH = 1.6 - 1.84 - 2.d
CF
J
-------
CALIBRATION CALCULATIONS METER BOX Calibrated by
Date 6 ",oO,"'}ci Box No.
0.0317 (Man. orifice) / (T + 460)*" \2
P. (OT, 4- 460)
b d
••' - ( '" • » + 460)
CF P. (T, avg. + 460)
w b d
CFd (P +
Man. orifice
13.6
(T + 460)
w
+ 460)
0.0368)
Man.
•5 l/.CO??
.JV-.?? x ,"': ''/.> ( 7^/ ' + 460)
,?'.. '.< C'A.'-•"+ 0.0735) ( ' >. + 460)
+ 460)
'"'/'•rV (,"'%:'''+ 0.147) ( ' -, +460)
5, -/I! x .'"•' '•'•'•'( "•'< + ^*60)
S,i,'-i .'.•> (' • - V+ 0.294) ( •'-••> +460)
i " ;n , " ' ""
C-v;1-! x ••'•>( /oo + 460)
i
* -> /,
| /.c><(( ('":. •"^+ 0,441) (; % + 460)
t
T-V'',x fOS'.S?( /rvl + 460)
H.r>-:') (."'? -.7+ 0.583) (/./••. +460)
i '
•> n
i . U
4.0
;
c. n
D . U
Q n
l,o.j(f ! ,
*
i '• ™ii~l "
• °° u.
'.0!JV
/ 'M ' *
AO; ->\
-------
Calibrated by
Date
Clean Quick Connects
Manoaeters
Iherno-eters
Lights
Electrical Check - Anphenol
7ariac
STACK SAMPLER CALIBRATION SHEET
-236-
Box No."
Leak Check at 27" Eg.' - Leakage
Remarks
?
Pu=p Oil
Valves
Dry Test Meter. ,
Buzzer
Vacuum Gau?,e
CFM
Bate
CALIBRATION - ORIFICE AND METER
Box No. j?AC.
Man
Orifice
CF
w
IT
0.5
1.0
2.0
4.0
6.0
2,
1L2M—
U-L&
8.0
f?
Calculate Y & AH* at can. 2.0
C
CF p (T, avg. + 460)
Y -
AH,
CF, (P + 0.147) (!„•+ 460)
db w
0.0634
(T + 460)
w
V
t \
P, (OT, +460)
o d
CF
Tolerances
Y « 0.99 - 1.00 - 1.01
AH - 1.6 - 1,84 - 2.1
d
avg .
Pb
s
3o./7
3/? /7 ! w
—Ji^xlUL,! !
10
37. ^
1*
10
10
-------
by
0.0317 (Man. orifice) /
-------
Pat..
-238-
Box
Bercraetric pressure, Pu = in. He
y
Dry gas neter Ho.
1
Orifice
manometer
settinq,
AH,
in. H20
0.5
1.0
2.0
4.0
6.0
8.0
Gas volume
vet test
meter
VH. %.
ft3 <
• -S.'CMI
5-^it
lOi^V'
Gas volume
dry gas
meter
Vd»
ft3
S.C%
Xlirg
/0,'jol
10<^<':j/^/Z.;5('
lOl^-
10t^
)0,1^
//),/3^
Temperature
Wet test! Dry gas raster
Meter
tw,
°F
*-i ^C I
7* /&
TIV-JV
-7^".^J
7^-
674-
W/rt
Inlet
^i*
°F
F2
?0
/^/
//O
' ,' "
/ / v
/•'^
Outlet
tdo*
°F
75^
-7?
*l
<; :',
^/
?^
Average
td.
*F
^4^
rl, ; \, 5 \t%
•^^ 1 \.ovHV
it-St | (.Dfi'b
;,^n 1 1,0? \i>
AHg
0.0317 L\( f(tw + 460) el2
QVQ/ W
\,^5
1-15^
|,1ll
1,1 K^ .
\,5l^
VSH:
Y s Ratio of accuracy of wet test meter to dry test meter. Tolerance = i 0.01
= Orifice pressure differential that gives 0.75 cfe of air at 70* F and 29.92
inches of mercury', in, ^0, Tolerance - - 0,15
Figure 9. Suggested orifice and dry gas meter calibration and calculation form.
-------
-239-
-------
-240-
Joe Wilson
VISIBLE EMISSIONS OBSERVER
QUALIFICATION RECORD
1
2
3
k
5
6
7
8
9
10
11
12
13
14
15*
16
17
18
19
20
21
22
23
24
25
Actual
Z
Opacity
QC
75
55
30
30
20
15
20
to
to
" 65
75
75 .
ho
35
35
25
25
20
20
20 , ,
20
30
30
60
TfEITE S!-!0:*E
Observer
Assigned
Opacity
100
75
50
30
25
20
15
20
1*0
to
70
80
85
50
Uo
35
25
20
15
15
20
15
hQ
U5
75
Etfror
5
0
5
0 '
5
0
0
0
0
0
5
5
10
10
5
°_J
0
5
5
5
0
5
| 10
15
15
1
Actual
a?
A
Opacity
95-'
95
80
70
75
60
60
'l»5
• to
to
20
25
20
15
• "15 1
20
25
30
*3Q
30
15
15
10
20
2-1
BLACK SMOKE
Observer
Assigned
Opacity
95
95
85
70
75
60
• 65
50
^5
. 35
20
25
20
15
20
25
15
15
20
20
15
10
10
10
10
Error
0
0
5
0 •
0
0
5 -
5
5
5
0
0
0
0
1 5
5
10
J
15 •
10
10
0
5
0
10 .
10
Test Date
Remarks
9/28/79
*r> *_ Y i •
Test Location
TECE.'OLOGY, II
Certified by: Joseph^Wilson__
Daniel F, FitzCerald
'or, "41 r> i net y
-------
J. Marino
-241-
VISIBLE EMISSIONS OBSERVER
QUALIFICATION RECORD
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22*
23
24
25
Actual
%
Opacity
95
100
85
so
65
60
50
Uo
^5
Ii5
35
30
25
20
15
15
20
55
60
25
20
15
15
20
1*5
WHITE SMOKE
Observer
Assigned
Opacity
90
90
85
80
70
70
60
liO
i»o
^5
30
25
20
20
. 20
20
30
^
55
20
15
15
15
15
30
Error
5
10
0
0
5
10
10
0
5
0
5
5
5
.0
5
5
10
10
5
5
5
0
0
5
15
i
!
Actual
%
Opacity
95
85
85
80
65
60
60
55
1»5
iiQ
30
25
30
25
20
30
30.
15
10
10
5
5
1 5
5
0
BLACK SMOKE
Observer
Assigned
Opacity
99
75
75
75
65
70
.. 60
55
' ^5
50
30
35
35
30
25
140
35
20
20
20
20
10
15
10
10
Error
5
- 10
10
5
0
10
0
0 .
0
10
0
10
5
L>
5
L P _
5
5
10
10 .
15
5
10
5
10
Test Date
Remarks
Test Location SCOT? Er/IHOin-lKirT
TECHNOLOGY, Ii;C., Plur3teacvilie,
Certified by; Jose?h Wilson
Daniel F. FitzGerald
Instructor
Division Manager
-------
Maynard Johnson.
-242-
VISIBLE EMISSIONS OBSERVER
QUALIFICATION RECORD
1
2
3
4
5
6
7
S
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
Actual
%
Opacity
85
90
90
85
. 85
80
75
70
70
40
50
55
40
25
25
20
25
25
25
15
25
10
5
5
5
WHITE SMOKE
Observer
Assigned
Opacity
95
90
85
80
75
70
65
60
60
45
40
50
40
25
30
20
20
25
30
15
20
20-
10
10
10
Error
10
0
5
5
10
,10
10
10
10
r
J
10
5
0
0
5
0
0
0
5
0
5
10
5
5
5
4
Actual
%
Opacity
90
90
' 85
65
70
70
65
65
50
30
25
20
15
20
20
10
10
15
10 J
10
10
5
5
5
5
BLACK SMOKE
Observer
Assigned
Opacity
95
85
80
60
65
70
75
70
50
30
35
20
15
25
15
10
15
15
10
15
10
15
10
5
5
Error
5
5
5
5
5
0
10
5
0
0
10 '
0
0
5
5
0
5
0
0
5
0
10
5
0
0
Test Date
Remarks
9/20/79
Test Location SCOTT ENVIRONMENTAL
TECHNOLOGY, INC., Plumstcadville, PA
Certified by: Joseph Wilson
Inst rue tor
Daniel J. FitzGerald
Division Manager
-------
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,^): ,v
STATE OF CALIFORNIA
AIK RESOURCES BOARD
This Certifies That
JJ-1
Has Attended The
VISIBLE EMISSION EVALUATION COURSE
OCTOBER 16
HOTTER
.to.
./
Qittf, Division of Legal Affairs arid Enforcomoiit
-------
12705-01-0380 -244"
APPENDIX F
SUPPLEMENTAL ANALYSIS
^_ Scott Environmental Technology inc.
-------
#2705-01-0380
-245-
SUPPLEF-iENTAL ANALYSIS
Four (4) ore samples were received by Scott during testing. These
were labeled Samples A-D. Laboratory analysis for moisture content as a
percent is summarized in Table F-l. The determination was made by taring
1000 ml beakers, weighing each sample and beaker to obtain initial sample
weight, heating the samples at 120 C to dry constant weight and calculating
moisture as a percent difference in the two weights for each sample,
TABLE F-l
MOISTURE RESULTS
Sample
Moisture %
A
1.16
B
0.99
C
13.52
D
13.12
210
£olj>rn urn .d^jiiP-Mlti VfijLJ)1!'1 ]i'sJjL
— k ^Q
Three probe washes and filters were analyzed for Po content by
Eberline Laboratories, Albuquerque, New Mexico. Results are presented below
in Table F-2.
TABLE F-2
Po210 RESULTS
Sample:
?i n
Po Content:
Drier
Cyclone
Inlet
27 ± 8
Drier
Scrubber
Inlet
38 ± 11
Drier
Scrubber
Outlet
0.0 ± 2.6
i Scott Environment a! Technology inc.
-------
#2705-01-0380
APPENDIX G
TRACE ELEMENT ANALYSIS
Sample #37689 - Grinder Cyclone Inlet, Run #2
Sample #37691 - Dryer Cyclone Inlet. North, Run #4
Sample #37692 - N/A
Sample #37693 - N/A
Scott Environmental Technology Inc
-------
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A.S.
-248-
CAPLC ADOfsESS "L£OOt7«ecJt, NM Jersey 07666 . Telephones: *ui ij/ '
;/ 2129470953
CONIflOl.A?iO r.;St*SCMCH:Ml3TKV. IMTRiJVtStAl ANO CNEMJCAL ANALYSIS * SAVHISO
V! = (C-HiS5. SHJF?£RS' RfWSCSTATIQN, st BEf 1CIATIG.S. M3 STOHACS OF DRES A-HO MttALS
REPORT OF ANALYSIS
No.
Our analysis of the sample of Dust Samples
From York Research Corporation
Marked: 15 Lots as below: P.O, #3-5830
• PARTS PER MILLTOr
and .'submitted to
us, snows:
i£i£j^Z.Mi £H§2i
COPPER — 50. 10. 5
NICKEL — 500. 100.
COBALT 20, -5.
i^cri ~ ——• - —- ' M M
MANGANESE -..— M 1000. "
CHROMIUM —— 500. 50.
VANADIUM „,.,-„— M M
TITANIUM — H M 2
SCANDIUM A A
CALCIUM —— M M
POTASSIUM M M
CHLORINE 200. 5C
SULFUR M .200.
PHOSPHORUS -— M 200.
SILICON -— M M
' ALUI-IINUM M M
MAGNESIUM . - A A
SODIUM — • M M
FLUORINE —-— 5. '2.
CARBON —
BORON • 500. - 100.
BERYLLIUM -,- —-— A A
LITHIUM — 20. ,20.
* $ ,«
< *= Less Than
A =* Matrix Interference
M = Signifies Major Constituent of Sample
To York Research Corporation
, (Page 3 of 12 Pages)
£3769.3
M •
100.
50.
M
•• 100.
50.
50.
500,
M
M
10.
M
50.
M
M '
A
M "
. 1.
200.
A
<0.5
LEDOUX & COMPANY
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EX 134340
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;;; • $.",;.-'U!>)j
rXUir.rAIIQ.V. SE.VtriCIATIO'i. t-.O Sl-jfi.'.SE Of C«rU #'JO K'TAIS
REPORT OF ANALYSI
No.
: analysis of the sample of Dust Samples
>m York Research Corporation
rked: 15 Lots ao below: P.O. #3-5830
and
PARTS PER HILLIC
PPRTTTM _
T f. yrrpu f, ;.:r I- T
Jj>U; iI1n!,U,-l —
RA r>TT":.-i
ppc' TTtr,i _
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Lots #37689
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#37691
50,
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500.
20.
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50.
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CAS"(ftv. ISiTSUWiriTAL AVO cPf'JCAL ASAtYjtS . 5.H!f>U.'i3
$mp?£ft$" Rti'KEssHr^Tiov. ScfieficiANO'i. *; P ~r f> ~ A r\j A f ^/ c-»cr
iw. i w i v i \~s : t~\i^ *-** L, i *.) t o
No.__ JPJA21:^
Our analysis of the sample of Dust Samples
From York Research Corporation
Marked: 15 lots as below: P.O. #3-5830
and
"I7~:
THORIUM — —— <10 <]..'
BISMUTH,—-—--——.•-
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