United States
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park NC 27711
EMB REPORT 81 -CBS-1
November & December 1981
Air
Coke Battery Stack
Sulfate Emissions
Emission Test Report
Republic Steel -
Cleveland Works
Cleveland, Ohio
VOLUME I
TEXT AND APPENDIX A
-------
SUMMARY TEST REPORT
Method Development and Testing for the
Coke Battery Stack Industry
Republic Steel-Cleveland Works
Volume I
Text and Appendix A
by
PEDCo Environmental, Inc.
11499 Chester Road
Cincinnati, Ohio 45246
Contract No. 68-02-3546
Work Assignment No. 10
ESED No. 74/4i
Task Manager
Frank Clay
Emission Measurement Branch, MD-13
Emission Standards and Engineering Division
U.S. ENVIRONMENTAL PROTECTION AGENCY
RESEARCH TRIANGLE PARK, NORTH CAROLINA 27711
December 1981
-------
CONTENTS
Figures iv
Tables vi
QA Element Finder xi
1. Introduction ' 1-1
2. Summary of Results 2-1
2.1 Particulate sampling protocol 2-1
2.2 Summary of particulate and related analyses
results 2-9
2.3 Comparison of particulate results at selected
temperature 2-41
2.4 Particulate sulfate 2-53
2.5 Discussion of particulate results 2-56
2.6 Discussion of back-half results 2-63
2.7 Reduced sulfur analysis by Method 15 2-64
2.8 Gas stream flow rate and composition 2-71
2.9 Visible emissions 2-79
2.10 Process data 2-83
3. Process Description 3-1
4. Sampling and Analytical Procedures 4-1
4.1 Sampling locations 4-1
4.2 Gas stream flow rate, temperature, and
composition 4-4
4.3 Particulate, sulfur dioxide, and sulfuric
acid mist emission tests 4-4
4.4 Reduced-sulfur emission tests 4-15
5. Quality Assurance 5-1
11
-------
CONTENTS (continued)
Appendices
A Computer Printouts and Example Calculations A-l
B Field Data B-l
C Laboratory Results C-l
D Sampling and Analytical Procedures D-l
E Calibration Procedures and Results E-l
F Quality Assurance F-l
G Project Participants and Project Log G-l
H Results of a Study to Evaluate Effects of Heating
on Filter Tare Weights H-l
I Midwest Research Institute Process Summary 1-1
111
-------
FIGURES
Number Page
2-1 Particulate Concentration vs. Average Actual
Filter Temperature During NCOG Underfiring 2-26
2-2 Particulate Concentration vs. Average Actual
Probe Temperature During DCOG Underfiring 2-27
2-3 Summary of Best-Fit Lines from Particulate
Concentration vs. Average Actual Filter
Temperature for NCOG and DCOG Underfiring 2-28
2-4 Average Percent Weight Loss from Sampling
Train 5, 121°C (250°F) Front-Half Tempera-
ture, Due to Heat Conditioning Prior to
Weighing (NCOG Underfiring) 2-45
2-5 Average Percent Weight Loss from Sampling
Train 5, 121°C (250°F) Front-Half Tempera-
ture, Due to Heat Conditioning Prior to
Weighing (DCOG Underfiring) 2-46
2-6 Comparison of Average Particulate Concentration
Determined from Sampling at the Specified
Temperature and from Sampling at 121°C (250°F)
and Analyzing After Sequentially Heating at
Specified Temperature for NCOG Underfiring
Conditions 2-57
2-7 Comparison of Average Particulate Concentration
Determined from Sampling at the Specified
Temperature and from Sampling at 121°C (250°F)
and Analyzing After Sequentially Heating at
Specified Temperatures for DCOG Underfiring
Conditions 2-58
2-8 Comparison of Average Particulate Concentration
from Actual Sampling Temperature, Sequential
Heating, and IPA Extraction for NCOG Under-
firing Conditions 2-60
IV
-------
FIGURES (continued)
Number Page
2-9 Comparison of Average Particulate Concentration
from Actual Sampling Temperature, Sequential
Heating, and IPA Extraction for DCOG Under-
firing Conditions 2-61
2-10 H0S Response Curve with Increasing Concentra-
tion 2-69
3-1 Process Flow Diagram, Republic Steel-Cleveland
Works 3-2
4-1 Coke Battery No. 1 Flue Gas Exit Stack 4-2
4-2 Coke Battery No. 1 Exit Stack Sampling Site
and Traverse Point Locations 4~3
v
-------
TABLES
Number Page
2-1 Summary of Sample Trains Temperature and Con-
figuration During NCOG Underfiring Testing 2-2
2-2 Summary of Sample Trains Temperature and Con-
figuration During DCOG Underfiring Testing 2-4
2-3 Comparison of Sample Train 5 Component Tem-
peratures During Standard Method 5 Sample
Collection 2-7
2-4 Summary of Results for NCOG Test Series (mg) 2-10
2-5 Summary of Results for DCOG Test Series (mg) 2-11
2-6 NCOG Underfiring Condition, Run No. 1 Test
Results (10/27/81) 2-12
2-7 NCOG Underfiring Condition, Run No. 2 Test
Results (10/27/81) 2-13
2-8 NCOG Underfiring Condition, Run No. 3 Test
Results (10/28/81) 2-14
2-9 NCOG Underfiring Condition, Run No. 4 Test
Results (10/28/81) 2-15
2-10 NCOG Underfiring Condition, Run No. 5 Test
Results (10/29/81) 2-16
2-11 NCOG Underfiring Condition, Run No. 6 Test
Results (10/29/81) 2-17
2-12 NCOG Underfiring Condition, Run No. 7 Test
Results (10/30/81) 2-18
2-13 NCOG Underfiring Condition, Run No. 8 Test
Results (10/30/81) 2-18
VI
-------
TABLES (continued)
Number Page
2-14 DCOG Underfiring Condition, Run No. Dl Test
Results (12/8/81) 2-19
2-15 DCOG Underfiring Condition, Run No. D2 Test
Results (12/10/81) 2-20
2-16 DCOG Underfiring Condition, Run No. D3 Test
Results (12/11/81) 2-21
2-17 DCOG Underfiring Condition, Run No. D4 Test
Results (12/12/81) 2-22
2-18 DCOG Underfiring Condition, Run No. D5 Test
Results (12/12/81) 2-23
2-19 DCOG Underfiring Condition, Run No. D6 Test
Results (12/13/81) 2-24
2-20 MCOG Underfiring Condition, Trains 1 and 2 of
Quad Train [121°C (250°F) Front Half] 2-29
2-21 NCOG Underfiring Condition, Trains 3 and 4 of
Quad Train [121°C (250°F) and 204°C (400°F)
Front Half] 2-30
2-22 NCOG Underfiring Condition, Train 5 [121°C
(250°F) Front Half] 2-31
2-23 NCOG Underfiring Condition, Train 6 [316°C
(600°F) Front Half] 2-34
2-24 DCOG Underfiring Condition, Trains 1 and 2 of
Quad Train [121°C (250°F) Front Half] 2-35
2-25 DCOG Underfiring Condition, Trains 3 and 4 of
Quad Train [177°C (350°F) and 204°C (400°F)
Front Half] 2-36
2-26 DCOG Underfiring Condition, Train 5 (121°C
(250°F) Front Half] 2-37
2-27 DCOG Underfiring Condition, Train 6 [316°C
(600°F) Front Half] 2-40
2-28 Results of Sequential Heating of Selected NCOG
Underfiring Test Series Samples 2-42
vn
-------
TABLES (continued)
Number Page
2-29 Results of Sequential Heating of Selected DCOG
Underfiring Test Series Samples 2-43
2-30 Results of Sequential Heating of Selected NCOG
Underfiring Test Series Run 8.5, Front Half 2-44
2-31 Comparison of Particulate Concentrations Deter-
mined from Sampling at Two Different Tempera-
tures Under NCOG Underfiring Conditions: 177°C
(350°F) vs. 121°C (250°F) but Analyzing After
Treatment at 177°C (350°F) 2-47
2-32 Comparison of Particulate Concentrations Deter-
mined from Sampling at Two Different Tempera-
tures Under NCOG Underfiring Conditions: 204°C
(400°F) vs. 121°C (250°F) but Analyzing After
Treatment at 204°C (400°F) 2-48
2-33 Comparison of Particulate Concentrations Deter-
mined from Sampling at Two Different Tempera-
tures Under NCOG Underfiring Conditions: 316°C
(600°F) vs. 121°C (250°F) but Analyzing After
Treatment at 315°C (600°F) 2-49
2-34 Comparison of Particulate Concentrations Deter-
mined from Sampling at Two Different Tempera-
tures Under DCOG Underfiring Conditions: 177°C
(350°F) vs. 121°C (250°F) but Analyzing After
Treatment at 177°C (350°F) 2-50
2-35 Comparison of Particulate Concentrations Deter-
mined from Sampling at Two Different Tempera-
tures Under DCOG Underfiring Conditions: 204°C
(400°F) vs. 121°C (250°F) but Analyzing After
Treatment at 204°C (350°F) 2-51
2-36 Comparison of Particulate Concentration Deter-
mined from Sampling at Two Different Tempera-
tures Under DCOG Underfiring Conditions: 316°C
(600°F) vs. 121°C (250°F) but Analyzing After
Treatment at 316°C (600°F) 2-52
2-37 Summary of Particulate and Acid Sulfate Results
for the NCOG Underfiring Test Series 2-54
2-38 Summary of Particulate and Acid Sulfate Results
for the DCOG Underfiring Test Series 2-55
Vlll
-------
TABLES (continued)
Number Page
2-39 Summary of Results Obtained Through Method 15
Analysis of SRU Inlet COG 2-65
2-40 Summary of Results Obtained Through Method 15
Analysis of SRU Outlet COG During DCOG
Underfiring 2-66
2-41 Summary of Results Obtained Through Method 15
Analysis of No. 1 Coke Battery Exit Stack Gas 2-67
2-42 Summary of Flue Gas Conditions During NCOG
Underfiring Testing 2-72
2-43 Summary of Flue Gas Conditions During DCOG
Underfiring Testing 2-75
2-44 Summary of Flue Gas Flow Rate and Temperature
as Measured by a Full Velocity Traverse 2-77
2-45 Summary of Visible Emissions Data No. 1 Coke
Battery Exit Stack, NCOG Underfiring Test
Series 2-80
2-46 NCOG Test Series Process Data 2-84
2-47 DCOG Test Series Process Data 2-85
2-48 Sulfur Content of Coal and Coke During NCOG
Tests (Percent) 2-86
2-49 Sulfur Content of Coal and Coke During DCOG
Tests (Percent) 2-86
4-1 NCOG Underfiring Test Series, October 26-30,
1981, Revised Sampling Schedule 4-5
4-2 DCOG Underfiring Test Series, December 7-13,
1981, Revised Sampling Schedule 4-6
4-3 NCOG and DCOG Underfiring Test Series Analyti-
cal Schedule 4-7
5-1 Field Equipment Calibration, Quad Train No. 1
(NCOG) 5~2
5-2 Field Equipment Calibration, Quad Train No. 2
(NCOG) 5-3
IX
-------
TABLES (continued)
Number Page
5-3 Field Equipment Calibration, Quad Train No. 3
(NCOG) 5-4
5-4 Field Equipment Calibration, Quad Train No. 4
(NCOG) 5-5
5-5 Field Equipment Calibration, Quad Train No. 5
(NCOG) 5-6
5-6 Field Equipment Calibration, Quad Train No. 6
(NCOG) 5-7
5-7 Field Equipment Calibration, Quad Train No. 1
(DCOG) 5-8
5-8 Field Equipment Calibration, Quad Train No. 2
(DCOG) 5-9
5-9 Field Equipment Calibration, Quad Train No. 3
(DCOG) 5-10
5-10 Field Equipment Calibration, Quad Train No. 4
(DCOG) 5-11
5-11 Field Equipment Calibration, Quad Train No. 5
(DCOG) 5-12
5-12 Field Equipment Calibration, Quad Train No. 6
(DCOG) 5-13
5-13 Field and Reagent Blank Analysis, NCOG Test
Series 5-14
5-14 Field and Reagent Blank Analysis, DCOG Test
Series 5-15
5-15 Summary of Results Obtained Through Method 15
Analysis of Audit Gases 5-17
x
-------
QA ELEMENT FINDER
Item
Project Description
Project Organization and
Responsibility
QA Objectives
Sampling Procedures
Sample Custody
Calibration Procedures
Analytical. Procedures
Data Validation, Reduction,
and Reporting
Internal QA Checks
Performance Systems Audits
Preventive Maintenance Schedule
Corrective Action
Quality Assurance Reports to
Management
Page
1-1
Appendix G
Appendix F, 5-1
Appendix D, 4-1
Appendix B and C
Appendix E
Appendix D, 4-1
Appendix F
Appendix F
Appendix F
Appendix F
Appendix F
Appendix F
XI
-------
SECTION 1
INTRODUCTION
During the weeks of October 26, 1981, and December 7, 1981,
PEDCo Environmental personnel conducted emission sampling pro-
grams at Republic Steel Corporation's Cleveland, Ohio, facility.
The primary objective of the field tests was to obtain data
on battery stack particulate emissions using several modifica-
tions of EPA Method 5. The modifications included front half
sampling train temperatures of 177°C (350°F), 204°C (400°F), and
316°C (600°F), post-test heating of samples and wet chemistry
analysis for sulfates. The data will be used, with other infor-
mation, to formulate a test method to measure total non-sulfate
particulate matter emissions from batteries underfiring non-
desulfurized coke oven gas (NCOG) and desulfurized coke oven gas
(DCOG); and, to determine the effect of underfiring NCOG and DCOG
on particulate emissions. The secondary objective of the field
tests was to measure the concentrations and types of reduced
sulfur compounds in the fuel gas before and after the Sulfiban
desulfurizer. Data on reduced sulfur compounds will be used,
along with other information, to determine the impact of desul-
furizers on sulfur compound emissions from coke ovens.
1-1
-------
The purpose of this test report is to describe the measure-
ment mode, document the results obtained, and discuss the pos-
sible relationships between the data and process or sampling
conditions.
Republic's Cleveland plant was selected as the test site for
the following reasons:
1. A pad up rebuilt of the battery was completed in 1977.
2. The plant uses no add-on pollution control devices at
the coke battery exhaust.
3. Earlier test data indicate that it is representative of
a well controlled facility.
4. The two test series could be conducted close enough in
time so as to reduce the effects of changes in condi-
tion of the battery on emissions.
Comprehensive testing was conducted at two sources:
0 The Coke Battery No. 1 exhaust
0 The Sulfiban sulfur removal unit (SRU)
At the final exit stack serving Coke Battery No. 1, particu-
late, sulfur dioxide, and sulfuric acid mist concentrations were
measured by EPA Methods 5 and 8* modified into a quad sampling
train arrangement and two single sampling trains. A test run
consisted of the operation of the quad train and two single
sampling trains. Sampling and analytical parameters were varied
between runs. Flue gas flow rates, temperature, moisture con-
tent, and composition [oxygen (CO and carbon dioxide (CO-)] were
measured in conjunction with the particulate test runs.
*
40 CFR 60,, Appendix A, Reference Methods 1 through 5 and 8,
July 1, 1981.
1-2
-------
Flue gas samples were collected at the inlet and outlet
(during DCOG testing only) of the Sulfiban desulfurization unit
for determination of hydrogen sulfide (H_S), carbonyl sulfide
(COS), carbon disulfide (CS2), and SO- concentrations. Gas
chromatographic (GC) separation and flame photometric detection
(FPD) by EPA Method 15* were used.
Visible emissions were observed at Coke Battery No. 1 exit
stack during particulate tests according to EPA Method 9.**
Midwest Research Institute (MRI) monitored process opera-
tions during both test series. Mr. Yogesh Doshi monitored the
NCOG test series, and Mr. Barry Gold monitored the DCOG test
series. Mr. Frank Clay, EPA Task Manager, observed the NCOG test
series, and Mr. Terry Harrison of EPA who represented Mr. Clay,
observed the DCOG test series.
40 CFR 60, Appendix A, Reference Method 15, July 1, 1981.
40 CFR 60, Appendix A, Reference Method 9, July 1, 1981.
1-3
-------
SECTION 2
SUMMARY OF RESULTS
This section presents the results from the normal coke oven
gas (NCOG) and desulfurized coke oven gas (DCOG) test series.
The NCOG test series was conducted during the week of October 26,
1981, and the DCOG test series during the week of December 7,
1981. The delay between the two test series was necessary to
allow the sulfur recovery unit (SRU) to stabilize after start-up.
2.1 PARTICULATE SAMPLING PROTOCOL
Tables 2-1 and 2-2 summarize sampling trains, configura-
tions, metered volumes, and component temperatures for the NCOG
and DCOG underfiring test series, respectively. Sampling Trains
1 through 4 comprised the quad train. Sampling Train 5 was the
standard Method 5 train, and Sampling Train 6 was equipped for
316°C (600°F) probe and filter heat. Back-half train configura-
tions and filter/probe temperatures varied between sample runs.
The sample identifications listed in Tables 2-1 and 2-2 gives the
sample train number (1 through 6), back-half configuration
(Method 8 or Method 5), and front-half probe/filter temperature
(°F).
Probe and filter temperatures were measured by thermocouples
that contacted a well that had been blown into the glass probe
2-1
-------
TABLE 2-1 . SUMMARY OF SAMPLE TRAINS TEMPERATURE AND CONFIGURATION
DURING NCOG UNDERFIRING TESTING
Run
1
i
o
c.
4
*T
(contini
Sampl e
identification
1-M8-250
2-M8-250
3-M8-350
4-M8-350
5-M5-250
6-M8-600
1-M8-250
2-M8-250
3-M8-400
4-M8-400
5-M5-250
6-M8-600
1-M8-250
2-M8-250
3-M8-350
4-M8-350
5-M5-250
6-M8-600
1-M8-250
2-M8-250
3-M8-400
4-M8-400
5-M5-250
6-M8-600
jed)
Date
(1981)
10/27
10/27
10/28
10/28
Metered9
vol ume
Nntf
1.76
1.67
1.68
1.64
1.44
1.42
1.59
1.50
1.46
1.44
1.50
1.65
1.75
1.66
1.63
1.58
1.72
1.84
0.99
0.88
0.93
0.85
2.18
1.11
dscf
62.21
58.98
59.28
57.95
50.97
49.99
56.00
52.91
51.50
50.79
52.92
58.42
61.88
58.55
57.66
55.81
60.90
64.99
34.78
30.89
32.97
30.05
76.86
39.14
Stack
temperature
°C
280
281
280
281
288
288
279
284
279
283
259
259
279
282
280
282
270
270
275
277
274
276
270
270
°F
537
538
536
538
550
550
535
543
534
542
499
499
535
540
536
540
518
518
527
531
525
529
518
518
Average probe
temperature
°C
126
126
211
239
123
334
124
122
203
210
114
332
125
129
186
191
109
334
127
125
248
138
112
336
°F
258
259
411
462
253
634
255
252
398
410
238
630
258
263
366
376
229
633
261
257
479
280
233
638
Average filter
temperature
°C
122
125
170
169
128
320
119
128
198
207
125
316
113
127
178
169
109
293
123
130
177
169
130
328
°F
252
257
338
336
263
608
247
263
389
404
257
600
236
260
353
336
229
560
254
266
350
337
266
622
to
I
to
-------
TABLE 2-1 (continued)
Run
5
6
7
8
Samp! e
identification
1-M8-250
2-M5-250
3-M8-350
4-M5-350
5-M5-250
6-M8-600
1-M8-250
2-M5-250
3-M8-400
4-M5-400
5-M5-250
6-M8-600
1-M8-250
2-M5-250
3-M8-350
4-M5-350
5-M5-400
6-M8-600
1-M8-350
2-M5-350
3-M8-400
4-M5-400
5-M8-250
6-M8-600
Date
(1981)
10/29
10/29
10/30
10/30
Metered
vol ume
Nm3
1.64
1.50
1.53
1.43
1.61
1.54
1.64
1.54
1.52
1.29
1.65
1.58
1.73
1.66
1.48
1.57
1.66
1.60
1.58
1.54
1.70
1.60
1.42
1.18
dscf
58.03
52.83
53.84
50.61
56.68
54.48
57.98
54.33
53.74
45.69
58.23
55.90
60.90
58.55
52.35
55.56
58.63
56.60
55.91
54.36
59.96
56.55
50.29
41.72
Stack
temperature
°C
274
276
276
275
271
271
274
277
277
278
271
271
277
280
277
280
271
271
285
283
285
286
271
271
°F
524
529
529
527
520
520
526
530
530
532
520
520
530
537
530"
536
520
520
545
542
545
547
520
520
Average probe
temperature
°C
124
127
184
178
129
325
127
121
203
196
118
328
122
130
131
169
208
329
182
184
208
214
128
326
°F
255
260
363
353
265
617
261
250
398
385
245
622
251
266
269
336
407
624
360
364
407
417
263
619
Average filter
temperature
°C
124
123
176
186
116
324
119
126
193
208
119
302
122
126
181
178
196
308
167
169
198
201
131
313
°F
255
254
349
366
240
616
246
258
379
407
246
576
252
258
358
353
385
587
332
336
388
393
268
596
to
I
CO
*
Metered volume in dry normal cubic meters (dNm ) and dry standard cubic feet (dscf)
tions = 20°C and 760 mmHg (68°F and 29.92 in.Hg) and zero percent moisture.
Standard condi-
-------
TABLE 2-2. SUMMARY OF SAMPLE TRAINS TEMPERATURE AND CONFIGURATION
DURING DCOG UNDERFIRING TESTING
Run
Dl
D2
D3
D4
Sampl e
identification
1-M8-250
2-M8-250
3-M8-350
4-M8-350h
5-M5-2500
6-M8-600
1-M8-250
2-M8-250
3-M8-350
4-M8-350
5-M5-250
6-M8-600
1-M8-250
2-M8-250
3-M8-400
4-M8-400
5-M5-250
6-M8-600
1-M8-250
2-M8-250
3-M8-400.
4-M8-400P
5-M5-250
6-M8-600
Date
(1981)
12/8
12/10
12/11
12/12
Metered3
vol ume
Nm3
1.25
1.23
1.16
1.12
0.96
1.40
1.78
1.71
1.79
1.84
1.68
1.48
1.62
1.40
1.44
1.79
1.72
1 1.69
1.69
1.49
1.75
1.67
dscf
44.11
39.67
40.99
39.61
34.02
49.40
62.68
60.47
63.26
64.79
59.35
52.29
57.25
49.32
51.01
63.10
60.82
59.82
59.79
52.50
61.80
58.85
Stack
temperature
°C
242
242
242
243
252
253
252
252
252
252
252
252
252
252
249
252
252
254
254
256
254
254
°F
468
468
468
470
485
487
486
486
486
486
486
486
486
486
480
486
486
490
490
492
490
490
Average probe
temperature
°C
129
124
178
175
265
238
237
186
173
129
320
127
125
214
218
124
325
113
123
207
134
302
°F
264
255
352
348
508
460
458
366
343
263
608
261
258
417
425
255
616
236
253
404
273
576
Average filter
temperature
°C
119
133
190
167
268
118
109
184
197
126
298
120
132
211
204
123
280
148
126
209
128
325
°F
246
272
374
333
515
244
229
363
387
258
569
248
270
411
400
254
536
299
259
409
263
617
(continued)
-------
TABLE 2-2 (continued)
Run
D5
D6
Sam pi e
identification
1-M8-250
2-M5-250
3-M8-350
4-M5-350
5-M5-250
6-M8-600
1-M8-250
2-M5-250
3-M8-400
4-M5-400
5-M5-250
6-M8-600
Date
(1981)
12/12
12/13
Metered
vol ume
Nm3
1.74
1.74
1.56
1.60
1.69
1.62
1.56
1.56
1.45
1.49
1.83
1.45
scf
61.31
61.44
55.07
56.59
59.67
57.09
54.92
54.96
51.23
52.62
64.63
51.10
Stack
temperature
°C
244
244
244
244
244
244
235
236
235
232
235
235
°F
471
471
471
471
471
471
455
457
455
449
455
455
Average probe
temperature
°C
120
123
177
178
132
327
121
127
211
204
125
324
°F
248
254
350
352
269
621
251
261
412
399
258
616
Average filter
temperature
°C
123
127
181
177
122
316
132
120
204
219
131
319
°F
253
261
357
351
251
600
270
248
399
427
267
607
to
I
1/1
Metered volume in dry normal cubic meters (dNm ) and dry standard cubic feet (dscf)
tions = 20°C and 760 mmHg (68°F and 29.92 in.Hg) and zero percent moisture.
DTest voided because of excessive post-test leak rate.
Standard condi-
-------
and the back-half of the glass filter holder. During a typical
EPA Method 5 test*, the filter box temperature is the only param-
eter monitored to control front-half heat. Table 2-3 summarizes
the sampling train component temperatures that were recorded
during all tests for Sampling Train 5. In this case, the stack
temperature was high 232° to 288°C (450° to 550°F), and the
sample gas stream temperature was reduced to the desired filter-
ing temperature. The filter box temperature and the actual
filter temperature compared closely.
Sampling was conducted isokinetically by regulating the
sample flow rate relative to the flue gas flow rate as measured
by the pitot tube attached to the probe assembly. Except for
Train 6 during NCOG underfiring, sampling trains were operated at
100 ^flO percent isokinetic. An oversized quartz glass nozzle and
a higher than expected grain loading prevented proper isokinetics
from being maintained throughout the entire scheduled sample run
on Train 6. During NCOG underfiring, Train 6 sampling rate
averaged 47 percent isokinetic. The oversized nozzle problem was
rectified for the DCOG underfiring test series.
Whatman Reeve Angel 934 AH glass fiber filters were used in
all sampling trains except Train 6, in which a quartz glass
filter was used. Filters were chosen for their proven tare
weight stability when subjected to the heat treatments in the
analytical procedures. Appendix H details a study conducted by
PEDCo to assess the effect of heat treatment on various filter
40 CFR 60, Appendix A, Reference Method 5, July 1, 1981.
2-6
-------
TABLE 2-3. COMPARISON OF SAMPLE TRAIN 5 COMPONENT TEMPERATURES
DURING STANDARD METHOD 5 SAMPLE COLLECTION
Test No.
1.5
2.5
3.5
4.5
5.5
6.5
8.5
D2.5
D3.5
D4.5
D5.5
D6.5
Average temperature, °C (°F)
Probe
123 (253)
114 (238)
109 (229)
112 (233)
129 (265)
118 (245)
128 (263)
129 (263)
124 (255)
134 (273)
132 (269)
125 (258)
Filter
128 (263)
125 (257)
109 (229)
130 (266)
116 (240)
119 (246)
131 (268)
126 (258)
123 (254)
128 (263)
122 (251)
131 (267)
Box
124 (256)
97 (207)
128 (263)
132 (270)
136 (277)
132 (270)
130 (267)
132 (270)
129 (264)
133 (271)
129 (264)
135 (275)
Stack
288 (550)
259 (499)
270 (518)
270 (518)
271 (520)
271 (520)
271 (520)
252 (486)
252 (486)
254 (490)
244 (471)
235 (455)
aTrain 7.5 operated at a higher temperature. Train D1.5 was a voided run.
Note: Probe, filter, and stack temperature measured by thermocouple
indicator. Box temperature measured by dial thermometer.
2-7
-------
tare weights. The Whatman Reeve Angel 934 AH proved to be one of
the most stable. As a matter of routine, all filters used in
this test program were heated at 316°C (600°F) prior to initial
tare weighing.
2-8
-------
2.2 SUMMARY OF PARTICULATE AND RELATED ANALYSES RESULTS
Tables 2-4 and 2-5 present the results obtained through
analysis of samples collected during the NCOG and DCOG test
series. All results are reported as milligrams (ing) . The ana-
lytical scheme used is presented in Section 4 and is discussed in
detail in Appendix D. Appendix C presents actual laboratory
data.
In addition to the particulate analysis, acetone rinse
residues and filters were analyzed for isopropanol soluble sul-
fate (acid sulfate) and water soluble sulfate (inorganic sul-
fate). Selected filters also were analyzed for total organic
carbon (TOO. Because the quantity of TOC proved to be negligi-
ble, the data were not included on the summary tables (refer to
Section 2.5.1 of this report for more information).
Back half solutions were analyzed for sulfuric acid mist and
sulfur dioxide by EPA Method 8 or inorganic and organic content
by ether/chloroform extraction and total organic carbon ampule
techniques depending on the back-half configuration.
Tables 2-6 through 2-13 present the analytical results for
each sampling train within a test run for NCOG underfiring, and
Tables 2-14 through 2-19 for DCOG underfiring. Analytical
results are reported in mg, milligrams per cubic meter (mg/m ),
and grains per dry standard cubic foot (gr/dscf). These tables
also present details on desired front-half temperature, on
average filter temperature, and on whether sequential heating of
the front-half samples was performed prior to sulfate analysis.
2-9
-------
TABLE 2-4. SUMMARY OF RESULTS FOR NCOG TEST SERIES (mg)
Run
No.
1.1
.2
.3
.4
.5
.6
2.1
2.2
2.3
2.4
2.5
2.6
3.1
3.2
3.3
3.4
3.5
3.6
4.1
4.2
4.3
4.4
4.5
4.6
5.1
5.2
5.3
5.4
5.5
5.6
6.1
6.2
6.3
6.4
6.5
6.6
7.1
7.2
7.3
7.4
7.5
7.6
8.1
8.2
8.3
8.4
8.5*
8.6
Filterable participates under various conditions (front-half results)
Ambient
temperature
Rinse
101.6
93.9
4 1.5
27.1
82.3
12.1
79.3
81.1
33.4
49.0
62.8
23.3
104.5
62.6
66.6
20.4
74.5
18.9
64.3
55.7
30.0
48.7
59.8
16.3
82.0
101.4
31.4
15.4
117.8
10.2
102.9
100.2
18.9
12.6
108.1
19.9
123.4
117.3
48.2
42.4
24.4
14.4
19.9
32.2
18.6
13.5
85.4
11.0
Filter
125.3
98.9
31.4
23.5
53.0
14.9
103.8
68.1
12.9
12.3
28.1
16.2
97.5
94.3
20.7
19.9
96.7
17.1
75.6
57.5
31.1
29.7
114.7
53.4
56.6
84.2
19.1
16.7
103.2
14.7
81.2
50.6
15.4
14.3
87.6
11.0
72.4
69.8
16.6
20.2
15.8
9.9
45.4
43.8
47.5
47.0
98.5
34.1
2-h at 350° F
Rinse
32.2
26.1
18.4
14.9
10.6
34.8
18.6
27.6
28.6
Filter
23.0
21.4
15.6
19.3
18.4
102.5
18.2
22.8
13.7
4-h at 350°F
Rinse
21.6
15.5
8.6
29.8
24.7
25.9
Filter
20.1
15.2
18.2
99.0
19.5
11.7
2-h at 400°F
Rinse
17.8
9.1
14.4
8.4
12.7
22.4
17.9
10.8
21.9
Filter
19.5
15.7
14.8
17.8
29.0
90.0
18.3
13.4
11.3
4-h at 400°F
Rinse
15.6
13.3
7.8
16.8
14.7
'19.8
Filter
18.9
14.4
17.4
87.9
17.6
10.5
2-h at 600°F
Rinse
12.5
10.3
5.6
14.0
10.9
16.5
Filter
18.0
12.2
16.4
85.0
16.8
9.3
IPA rinse
(H2S04)
Rinse
38.2
7.4
9.8
2.1
0.0
0.0
35.1
0.0
12.2
14.4
0.0
2.6
40.5
0.0
24.1
3.7
0.0
4.2
23.0
0.4
6.4
10.0
0.0
0.0
65.5
3.0
9.5
0.0
0.0
0.0
47.6
0.0
2.8
0.0
0.0
0.0
Filter
43.3
0.0
0 0
z'.l
0.0
0.0
26.5
0.0
0.0
0.0
0.0
0.0
29.9
0.0
1.2
0.0
0.0
0.0
24.5
0.0
0.0
2.6
0.0
0.0
20.1
0.0
0.0
0.0
0.0
0.0
23.4
0.0
0.0
0.0
0.0
0.0
H?0 rinse
Rinse
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Filter
0
0
n
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0 .
0
Back-half results
S02
1960
1850
1S7Q
1810
1120
1370
1720
1700
1610
1940
1790
1540
1680
1620
1720
1300
1170
1250
1160
1550
2070
1970
2050
2000
1900
2010
H2S04
8.89
9.43
65.4
56.0
606
741
16.0
53.0
19.6
15.7
8.3
8.6
67.2
89.2
164
11.5
11.9
29.8
10.4
73.7
34.4
81.5
129
24.0
97.6
115
Ether chloroform
Inorganic
28.2
68.2
99.1
65.7
19.0
101.2
20.9
109.7
118.3
20.0
Organic
2.6
4.8
3.2
3.1
4.2
3.2
6.3
4.0
5.9
6.4
TOC
23.4
44.3
77.3
14.3
58.1
49. Z
11.8
42.3
15.4
15.2
rO.
M
O
Special sequential analysis performed.
-------
TABLE 2-5. SUMMARY OF RESULTS FOR DCOG TEST SERIES (mg)
Run
No.
01.1
01.2
01.3
01.4,
01. 5a
01.6
02.1
02.2
02.3
02.4
02.5
02.6
03.1
03.2
03.3
03. 4
03.5
03.6
04. 1
04.2
04.3
04.4*
04.5
04.6
05.1
05.2
05.3
05.4
05. 5
05.6
06.1
06.2
06.3
06.4
06.5
06.6
Filterable participates under various conditions (front-half results)
Ambient
temperature
Rinse
18.0
22.2
17.2
23.6
15.2
242. 8b
25.1
21.0
25.9
24.4
14.7
26.8
19.4
18.3
27.4
18.9
16.7
18.3
36.9
16.4
19.6
12.2
17.8
14.8
11.0
15.1
9.5
7.9
7.2
14.2
10.8
8.0
12.6
6.8
Filter
14.6
15.2
16.8
19.7
12.1
7.2
13.2
13.8
11.3
16.7
15.6
11.8
15.1
12.6
11.3
16.1
8.8
10.2
8.3
8.4
11.6
5.3
5.5
5.2
5.3
4.0
6.4
5.0
5.0
6.9
4.8
4.0
7.3
2.4
2-h at 350=F
Rinse
8.4
7.5
12.5
11.0
7.3
13.4
5.6
2.6
8.4
Filter
13.4
14.5
12.1
12.4
14.9
8.3
3.1
4.3
5.2
q-n ai JDUT
Rinse
7.9
9.3
6.0
13.1
2.5
7.8
Filter
13.2
9.9
13.9
7.1
2.8
5.0
-n a i HW r
Rinse
5.4
8.9
6.3
5.3
8.1
7.6
2.5
1.7
6.5
Filter
11.4
9.9
11.8
10.4
5.4
7.5
2.0
3.7
5.0
H-II OL HUU r
Rinse
5.4
8.0
5.3
7.6
2.5
6.5
Filter
11.0
9.7
10.4
7.3
2.0
4.8
2-h st SCC°F
Rinse
3.8
6.2
4.2
6.0
1.4
1.0
Filter
10.8
8.9
9.2
6.3
1.0
3.4
IPA rinse
(H?SOi)
Rinse
0.0
1.0
0.0
0.0
0.0
1.0
1.3
0.6
0.4
0.0
0.0
0.3
0.1
0.0
1.9
0.0
0.0
0.0
0.0
0.7
0.0
0.0
3.4
0.6
2.2
0.6
0.0
0.3
0.0
0.0
1.0
0.0
0.0
0.2
Filter
0.0
1.0
0.0
0.0
0.0
0.0
1.3
0.0
0.0
0.0
<0.3
0.0
1.7
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
HZ0 rinse
Rinse
0.0
2.1
2.5
0.0
1.6
0.9
2.0
3.5
4.8
0.0
0.0
6.0
0.0
4.1
0.8
0.9
2.2
0.0
0.9
3.2
0.0
0.0
3.7
1.7
1.6
3.8
0.0
1.4
0.0
0.0
0.0
0.0
0.0
0.0
Filter
<0.3
Void
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
<0.3
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Back-half results
S02
69.7
116.1
117.0
115.8
97.9
120.8
159.4
155.0
131.8
152.8
90.1
152.8
130.8
143.4
169.1
135.6
130.5
118.3
90.1
131.8
123.6
129.0
118.3
113.3
110.1
H2S04
115
3.5
9.3
9.2
6.3
13.7
14.4
8.7
54.8
10.7
84.0
7.0
12.0
8.2
12.8
42.3
15.9
6.7
74.7
8.8
7.8
8.2
13.2
r
7.5
11.4
rthar- rtilnmfnm
Inorganic
_
152.6
28.9
84.5
74.5
158.1
15.6
55.2
144.2
10.0
Organic
_
0.8
2.0
2.9
0.7
4.0
1.4
2.4
2.8
2.4
TOC
—
8.6
3.4
8.5
202
572
3.6
403
77
8.0
to
I
Test run voided.
bContam1nated with oil.
-------
TABLE 2-6. NCOG UNDERFIRING CONDITION, RUN NO. 1
TEST RESULTS (10/27/81)
Desired front-half tem-
perature. °C (CF)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C (°F)
Front-half catch
Particulate (ambient)
mg ,
mq/m
gr/dscf
Acid soluble sulfate
as [H2S04]
mg ,
mg/m
gr/dscf
as [H2S04(H20)2]
mg ,
mg/m
gr/dscf
Back-half catch
Su'lfuric acid mist
mg ,
mg/m
gr/dscf
ppm
Sulfur dioxide
mg 3
mg/m
gr/dscf
ppm
Inorganic condensibles
mg 3
mg/m
gr/dscf
Organic condensibles
mg 3
mg/m
gr/dscf
Total organic carbon
mg 3
mg/m
gr/dscf
1.1
121
(250)
122
(252)
226.9
128.9
0.056
81.5
46.3
0.020
111.4
63.3
0.028
8.9
5.0
0.002
1
1960
1114
0.486
419
1.2
121
(250
125
(257)
177
(350)
192.8
115.4
0.050
7.4
4.4
0.002
10.1
6.1
0.003
9.4
5.6
0.002
1
1850
1108
0.484
416
Test
1.3
177
(350)
170
(338)
72.9
43.4
0.019
9.8
5.8
0.002
13.4
8.0
0.003
65.4
38.9
0.017
10
1870
1113
0.487
418
No.
1.4
177
(350)
169
(336)
50.6
30.8
0.013
4.7
2.9
0.001
6.4
3.9
0.002
56.0
34.1
0.015
8
1810
1104
0.482
415
1.5
121
(250)
128
(263)
316
(600)
135.3
94.0
0.041
0.0
0.0
0.000
0.0
0.0
0.000
28.2
19.6
0.008
2.6
1.8
0.001
23.4
16.2
0.007
1.6
316
(600)
320
(608)
27.0
19.0
0.008
0.0
0.0
0.000
0.0
0.0
0.000
606a
426.8
0.187
105
1120
789
0.346
296
'Hydrogen peroxide contaminated.
2-12
-------
TABLE 2-7. NCOG UNDERFIRING CONDITION, RUN NO. 2
TEST RESULTS (10/27/81)
Desired front-half tem-
perature, °C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C (°F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04]
M9 3
mg/m
gr/dscf
as [H2S04 (H20)2]
ir.g 3
irg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mg 3
nig/m
gr/dscf
ppm
Sulfur dioxide
mg 3
mg/m
cir/dscf
ppm
Inorganic condensibles
nig .
ng/m
gr/dscf
Organic condensibles
mg 3
rng/m
ijr/dscf
Totil organic carbon
mg 3
mg/m
ijr/dscf
Test No.
2.1
121
(250)
119
(247)
183.1
115.2
0.050
61.6
38.7
0.017
84.2
53.0
0.023
741a
466
0.204
114
1370
862
0.377
324
2.2
121
(250)
128
(263)
204
(400)
149.2
99.5
0.044
0.0
0.0
0.000
0.0
0.0
0.000
16.0
10.7
0.005
3
1720
1147
0.502
431
2.3
204
(400)
198
(389)
46.3
31.7
0.014
12.2
8.3
0.004
16.7
11.4
0.005
53.0
36.3
0.016
9
1700
1164
0.509
438
2.4
204
(400)
207
(404)
61.3
42.6
0.019
14.4
10.0
0.004
19.7
13.7
0.006
19.6
13.6
0.006
3
1610
1118
0.489
420
2.5
121
(250)
125
(257)
316
(600)
90.9
60.6
0.026
0.0
0.0
0.000
0.0
0.0
0.000
68.2
45.5
0.020
4.8
3.2
0.001
44.3
29.5
0.013
2.6
316
(600)
316
(600)
39.5
23.9
0.010
2.6
1.6
0.001
3.5
2.1
0.001
157
95.7
0.041
23
1940
1176
0.512
442
aHydnogen peroxide contaminated.
2-13
-------
TABLE 2-8. NCOG UNDERFIRING CONDITION, RUN NO. 3
TEST RESULTS (10/28/81)
Desired front-half tem-
perature, "C (CF)
Actual average filter
temperature. "C (°F)
Sequential heating,
°C (°F)
Front-half catch
Paniculate (ambient)
mg ,
mg/m
gr/dscf
Acid soluble sulfate
as [H.SO.]
ng 3
rng/m
gr/dscf
as [H2S04(H20)2]
ing ,
mg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mg -
mg/m
gr/dscf
ppm
Sulfur dioxide
mg -
mg/m
gr/dscf
ppm
Inorganic condensibles
mg ,
mg/m
gr/dscf
Organic condensibles
mg ,
mg/irr
gr/dscf
Total organic carbon
mg ,
mg/m
gr/dscf
Test No.
3.1
121
(250)
113
(236)
202.0
115.4
0.050
70.4
40.2
0.017
96.2
55.0
0.024
8.3
4.7
0.002
1
1790
1023
0.446
384
3.2
121
(250)
127
(260)
177
(350)
156.9
94.5
0.041
0.0
0.0
0.000
0.0
0.0
0.000
8.6
5.2
0.002
1
1540
928
0.406
349
3.3
177
(350)
178
(353)
87.3
53.6
0.023
25.3
15.5
0.007
34.6
21.2
0.009
67.2
41.2
0.018
10
1680
1031
0.450
387
3.4
177
(350)
169
(336)
40.3
25.5
0.011
3.7
2.3
0.001
5.0
3.2
0.001
89.2
56.4
0.025
14
1620
1025
0.448
385
3.5
121
(250)
109
(229)
316
(600)
171.2
99.5
0.043
0.0
0.0
0.000
0.0
0.0
0.000
99.1
57.6
0.025
3.2
1.9
0.001
77.3
44.9
0.020
3.6
316
(600)
293
(560)
36.0
19.6
0.008
4.2
2.3
0.001
5.7
3.1
0.001
164
89.1
0.039
22.
1720
935
0.408
351
2-14
-------
TABLE 2-9. NCOG UNDERFIRING CONDITION, RUN NO. 4
TEST RESULTS (10/28/81)
Desired front-half tem-
perature, "C (BF)
Actual average filter
temperature, 6C (°F)
Sequential heating,
°c I;°F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04]
mg 3
mg/m
gr/dscf
as [H2S04(H20)2]
mg »
mg/m
gr/dscf
Back-half catch
Sulfurlc acid mist
mg ,
mg/m
gr/dscf
ppm
Sulfur dioxide
mg ,
mg/m
gr/dscf
ppm
Inorganic condensibles
mg ,
mg/nr
gr/dscf
Organic condensibles
mg 3
mg/m
gr/dscf
Total organic carbon
mg ,
mg/m
gr/dscf
Test No.
4.1
121
(250)
123
(254)
139.9
141.3
0.062
47.5
47.9
0.021
64.9
65.6
0.029
11.5
11.6
0.005
3
1300
1313
0.577
494
4.2
121
(250)
130
(266)
204
(400)
113.2
128.6
0.056
0.4
0.4
0.0002
0.5
0.6
0.0002
11.9
13.5
0.006
3
1170
1329
0.584
500
4.3
204
(400)
177
(350)
61.1
65.7
0.028
6.4
6.9
0.003
8.7
9.4
0.004
29.8
32.0
0.014
8
1250
1344
0.585
505
4.4
204
(400)
169
(337)
78.4
92.2
0.040
12.6
14.8
0.006
17.2
20.3
0.009
10.4
12.2
0.005
3
1160
1365
0.596
513
4.5
121
(250)
130
(266)
316
(600)
174.5
80.0
0.035
0.0
0.0
0.000
0.0
0.0
0.000
65.7
30.1
0.013
3.1
1.4
0.0001
14.3
6.6
0.003
4.6
316
(600)
328
(622)
69.7
62.8
0.027
0.0
0.0
0.000
0.0
0.0
0.000
73.7
66.4
0.029
16
1550
1396
0.611
525
2-15
-------
TABLE 2-10. NCOG UNDERFIRING CONDITION, RUN NO. 5
TEST RESULTS (10/29/81)
Desired front-half tem-
peniture, °C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C C'F)
Front- ha If catch
Partlculate (ambient)
ing 3
mg/m
!)r/dscf
Add soluble sulfate
as [H2S04]
In9 3
mg/m
gr/dscf
as [H2S04(H20)2]
mg ,
mg/m
gr/dscf
Back-half catch
Sulfurlc acid mist
img ,
mg/m
gr/dscf
ppm
Sulfur dioxide
mg -
mg/m
gr/dscf
ppm
Inorganic condensibles
mg ,
mg/m
gr/dscf
Organic condensibles
mg 3
mg/m
gr/dscf
Total organic carbon
mg ,
mg/m
gr/dscf
Test No.
5.1
121
(250)
124
(255)
138.6
84.5
0.037
85.6
52.2
0.023
117.0
71.3
0.031
34.4
21.0
0.009
5
2070
1262
0.550
474
5.2
121
(250)
123
(254)
177
(350)
185.6
123.7
0.054
3.0
2.0
0. 0008
4.1
2.7
0.001
19.0
12.7
0.006
4.2
2.8
0.001
58.1
38.7
0.017
5.3
177
(350)
176
(345)
50.5
33.0
0.014
9.5
6.2
0.003
13.0
8.5
0.004
81.5
53.3
0.023
13
1970
1288
0.564
484
5.4
177
(350)
186
(366)
32.1
22.4
0.010
0.0
0.0
0.000
0.0
0.0
0.000
101.2
70.8
0.031
3.2
2.2
0.001
49.2
34.4
0.015
5.5
121
(250)
116
(240)
316
(600)
221.0
137.3
0.060
0.0
0.0
0.000
0.0
0.0
0.000
20.9
13.0
0.006
6.3
3.9
0.002
11.8
7.3
0.003
5.6
316
(600)
324
(616)
24.9
16.2
0.007
0.0
0.0
0.000
0.0
0.0
0.000
129
83.8
0.036
20
2050
1331
0.581
500
2-16
-------
TABLE 2-11. NCOG UNDERFIRING CONDITION, RUN NO. 6
TEST RESULTS (10/29/81)
Desired front-half tem-
perature, "C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating.
Front-half catch
Paniculate (ambient)
mg ,
mg/m
gr/dscf
Acid soluble sulfate
as [H?SOJ
"9 3
mg/m
gr/dscf
as [H.S04(H20)2]
""9 3
mg/m
gr/dscf
Back-half catch
Sulfurlc add mist
mg ,
mg/m
gr/dscf
l>pm
Sulfur dioxide
rug ,
rng/m
gr/dscf
ppm
Inorganic condenslbles
mg ,
mg/m
gr/dscf
Organic condenslbles
mg .
mg/m
gr/dscf
Total organic carbon
mg _
mg/m
gr/dscf
Test No.
6.1
121
(250)
119
(246)
184.1
112.2
0.049
71.0
43.3
0.019
97.0
59.2
0.026
24.0
14.6
0.006
4
2000
1219
0.532
458
6.2
121
(250)
126
(258)
204
(400)
150.8
97.9
0.043
0.0
0.0
0.000
0.0
0.0
0.000
109.7
71.2
0.031
4.0
2.6
0.001
42.3
27.5
0.012
6.3
204
(400)
193
(379)
34.3
22.6
0.010
2.8
1.8
0. 0008
3.8
2.5
0.001
97.6
64.2
0.028
16
1900
1250
0.546
470
6.4
204
(400)
208
(407)
26.9
20.8
0.009
0.0
0.0
0.000
0.0
0.0
0.000
118.3
91.7
0.040
5.9
4.6
0.002
154a
119.4
0.052
6.5
121
(250)
119
(246)
316
(600)
195.7
118.6
0.052
0.0
0.0
0.000
0.0
0.0
0.000
20.0
12.1
0.005
6.4
3.9
0.002
15.2
9.2
0.004
6.6
316
(600)
302
(5760
30.9
19.6
0.008
0.0
0.0
0.000
0.0
0.0
0.000
115
72.8
0.032
18
2010
1272
0.555
478
'Contaminated with Isopropanol.
2-17
-------
TABLE 2-12. NCOG UNDERFIRING CONDITION, RUN NO. 7 TEST RESULTS (10/30/81)
Desired front-half tem-
perature, °C (°F)
Actual average filter
temperature, °C (°F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
Test No.
7.1
121
(250)
122
(252)
195.8
113.2
0.050
• 7.2
121
(250)
126
(258)
187.1
112.7
0.049
7.3
177
(350)
181
(358)
64.8
43.8
0.019
7.4
177
(350)
178
(353)
62.6
39.9
0.017
7.5
204
(400)
196
(385)
40.2
24.2
0.010
7.6
316
(600)
308
(587)
24.3
15.2
0.007
TABLE 2-13. NCOG UNDERFIRING CONDITION, RUN NO. 8 TEST RESULTS (10/30/81)
Test No.
Desired front-half tem-
perature, °C (°F)
Actual average filter,
perature, °C (°F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
8.1
177
(350)
167
(332)
65.3
41.3
0.018
8.2
177
(350)
169
(336)
76.0
49.4
0.022
8.3
204
(400)
198
(388)
66.1
38.9
0.017
8.4
204
(400)
201
(393)
60.5
37.8
0.016
8.5
121
(250)
131
(268)
183.9
129.5
0.056
8.6
316
(600)
313
(596)
45.1
38.2
0.017
2-18
-------
TABLE 2-14. DCOG UNDERFIRING CONDITION, RUN NO. Dl TEST RESULTS (12/8/81)
Desired front- half tem-
perature, °C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C (°F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04(H20)2]
mg 3
mg/m
gr/dscf
Water soluble sulfate
as [S04=]
mg 3
mg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mg 3
mg/m
gr/dscf
ppm
Sulfur dioxide
mg 3
mg/m
gr/dscf
ppm
Test No.
Dl.l
121
(250)
119
(246)
316
(600)
32.6
26.1
0.011
0.0
0.0
0.000
<0.3
<0.2
<0.0001
11 5a
92.0
0.040
22
69.7
55.8
0.024
21
D1.2
121
(250)
133
(272)
177
(350)
37.4
33.4
0.014
2.7
2.4
0.001
2.1
1.9
0.001
3.5
3.1
0.001
1
116.1
103.7
0.045
39
D1.3
177
(350)
190
(374)
34.0
29.3
0.013
0.0
0.0
0.000
2.5
2.1
0.001
9.3
8.0
0.004
2
117.0
100.9
0.044
38
D1.4
177
(350)
167
(333)
43.3
38.7
0.017
0.0
0.0
0.000
0.0
0.0
0.000
9.2
8.2
0.004
2
115.8
103.4
0.045
39
D1.5
Void
D1.6
316
(600)
268
(515)
27.3
28.4
0.012
0.0
0.0
0.000
1.6
1.7
0.001
6.3
6.6
0.003
2
97.9
102.0
0.044
38
Hydrogen peroxide contaminated.
2-19
-------
TABLE 2-15. DCOG UNDERFIRING CONDITION, RUN NO. D2 TEST RESULTS (12/10/81)
Desired front-half tem-
perature. °C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
8C (°F)
Front-half catch
Partlculate (ambient)
mg ,
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04(H20)2]
mg 3
mg/m
gr/dscf
Water soluble sulfate
as [S04«]
mg 3
mg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mg .
mg/m
gr/dscf
ppm
Sulfur dioxide
mg ,
mg/m
gr/dscf
ppm
Inorganic condensibles
mg -
mg/m
gr/dscf
Organic condensibles
mg -
mg/m
gr/dscf
Total organic carbon
mg ,
mg/m
gr/dscf
Test No.
D2.1
121
(250)
118
(244)
249.9*
178.5
0.078
1.4
1.0
0.0004
0.9
0.6
0.0003
13.7
9.8
0.004
2
120.8
86.3
0.038
32
D2.2
121
(250)
109
(229)
177
(350)
38.3
21.5
0.009
3.5
2.0
0.001
2.0
1.1
0.001
14.4
8.1
0.004
2
159.4
89.6
0.039
34
D2.3
177
(350)
184
(363)
34.8
20.4
0.009
0.8
0.5
0.0001
3.5
2.0
0.001
8.7
5.1
0.002
1
155.0
90.6
0.040
34
02. 4
177
(350)
197
(387)
37.2
20.8
0.009
0.5
0.3
0.0001
4.8
2.7
0.002
54. 8b
30.6
0.013
8
131.8
73.6
0.032
28
02. 5
121
(250)
126
(258)
316
(600)
41.1
22.3
0.010
0.0
0.0
0.000
0.0
0.0
0.000
152.6
82.9
0.036
0.8
0.43
0.0002
8.6
4.7
0.002
D2.6
316
(600)
298
(569)
30.3
18.0
0.008
<0.4
<0.2
<0.0001
<0.3
<0.2
<0.0001
10.7
6.4
0.003
2
152.8
91.0
0.040
34
Acetone rinse contaminated with oil.
Hydrogen peroxide contaminated.
2-20
-------
TABLE 2-16. DCOG UNDERFIRING CONDITION, RUN NO. D3
TEST RESULTS (12/11/81)
Desired front-half tem-
perature, °C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C (»F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04(H20)2]
mg 3
mg/m
gr/dscf
Water soluble sulfate
as IS04=]
' m9 3
mg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mg 3
mg/m
gr/dscf
Ppm
Sulfur dioxide
mg ,
mg/m
gr/dscf
ppm
Inorganic condensibles
mg 3
mg/m
gr/dscf
Organic condensibles
mg -
mg/m
gr/dscf
Total organic carbon
mg ,
mg/m
gr/dscf
Test No.
D3.1
121
(250)
120
(248)
38.6
26.1
0.011
0.4
0.3
0.0001
6.0
4.0
0.002
84. Oa
56.8
0.025
14
90.1
60.9
0.026
23
03. 2
121
(250)
132
(270)
204
(400)
34.5
21.3
0.009
2.5
1.5
0.001
0.0
0.0
0.000
7.0
4.3
0.002
1
152.8
94.3
0.041
35
03. 3
204
(400)'
211
(411)
30.9
22.1
0.010
0.0
0.0
0.000
4.1
2.9
0.002
12.0
8.6
0.004
2
130.8
93.4
0.041
35
D3.4
204
(400)
204
(400)
38.7
26.9
0.012
2.6
1.8
0.001
0.8
0.5
0.0003
8.2
5.7
0.002
1
143.4
99.6
0.043
37
03. 5
121
(250)
123
(254)
316
(600)
35.0
19.6
0.008
0.0
0.0
0.000
0.9
0.5
0.0002
28.9
16.1
0.007
2.0
1.1
0.0005
3.4
1.9
0.0008
D3.6
316
(600)
280
(536)
25.5
14.8
0.006
0.0
0.0
0.000
2.2
1.3
0.001
12.8
7.4
0.003
2
169.1
98.3
0.043
37
Hydrogen peroxide contaminated.
2-21
-------
TABLE 2-17. DCOG UNDERFIRING CONDITION, RUN NO. D4 TEST RESULTS (12/12/81)
Desired front-half tem-
perature, "C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C (°F)
Front-half catch
Particulate (ambient)
mg ,
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04(H20)2]
mg 3
mg/m
gr/dscf
Mater soluble sulfate
as [S04°]
mg ,
mg/m
gr/dscf
Back-half catch
Sulfuric add mist
mg ,
mg/m
gr/dscf
PPm
Sulfur dioxide
mg 3
mg/m
gr/dscf
ppm
Inorganic condensibles
mg -
mg/m
gr/dscf
Organic condensibles
mg ,
mg/m
gr/dscf
Total organic carbon
mg ,
mg/m
gr/dscf
Test No.
04. 1
121
(250)
148
(299)
28.5
16.9
0.007
0.0
0.0
0.000
0.0
0.0
0.000
42.3s
25.0
0.011
6
135.6
80.2
0.035
30
04. 2
121
(250)
126
(259)
204
(400)
45.2
26.7
0.012
0.0
0.0
0.000
0.9
0.5
0.0002
15.9
9.4
0.004
2
130.5
77.2
0.034
29
04.3
204
(400)
209
(409)
24.8
16.6
0.007
0.9
0.6
0.0003
3.2
2.1
0.001
6.7
4.5
0.002
1
118.3
79.4
0.035
30
04. 4
Void
04. 5
121
(250)
128
(263)
316
(600)
31.2
17.8
0.008
0.0
0.0
0.000
0.0
0.0
0.000
84.5
48.3
0.021
2.9
1.6
0.0007
8.5
4.8
0.002
04. 6
316
(600)
325
(617)
17.5
10.5
0.004
0.0
0.0
0.000
0.0
0.0
0.000
74. 7a
44.7
0.020
11
90.1
54.0
0.024
20
'Hydrogen peroxide contaminated.
2-22
-------
TABLE 2-18. DCOG UNDERFIRING CONDITION, RUN NO. D5 TEST RESULTS (12/12/81)
Desired front-half tem-
perature, °C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C (°F)
Front-half catch
Particulate (ambient)
mg .
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04 (H20)2]
mg -
mg/m
gr/dscf
Water soluble sulfate
as [S04=]
mg ,
mg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mg ,
mg/m
gr/dscf
ppm
Sulfur dioxide
mg ,
mg/m
gr/dscf
ppm
Inorganic condensibles
1119 , 3
mg/m
gr/dscf
Organic condensibles
mg, 3
mg/m
gr/dscf
Total organic carbon
mg -
mg/m
gr/dscf
Test No.
D5.1
121
(250)
123
(253)
23.3
13.4
0.006
4.6
2.6
0.001
3.7
2.1
0.001
8.8
5.0
0.002
1
131.8
75.7
0.033
28
D5.2
121
(250)
127
(261)
177
(350)
20.0
11.5
0.005
1.1
0.6
0.0003
1.7
1.0
0.001
74.5
42.8
0.019
0.70
0.40
0.0002
202a
116
0.050
D5.3
177
(350)
181
(357)
16.3
10.4
0.004
3.0
1.9
0.001
1.6
1.0
0.0004
7.8
5.0
0.002
1
123.6
79.2
0.035
30
D5.4
177
(350)
177
(351)
19.1
11.9
0.005
0.8
0.5
0.0002
3.8
2.4
0.001
158.1
98.8
0.043
4.0
2.5
0.001
572a
357
0.156
D5.5
121
(250)
122
(251)
316
(600)
15.9
9.4
0.004
0.0
0.0
0.000
0.0
0.0
0.000
15.6
9.2
0.004
1.4
0.83
0.0004
3.6
2.1
0.0009
05. 6
316
(600)
316
(600)
12.9
3.0
0.003
0.4
0.2
0.0001
1.4
0.9
0.0003
8.2
5.1
0.002
1
129.0
79.6
0.035
30
Contaminated with isopropanol.
2-23
-------
TABLE 2-19. DCOG UNDERFIRING CONDITION, RUN NO. D6 TEST RESULTS (12/13/81)
Desired front-half tem-
perature, °C (°F)
Actual average filter
temperature, °C (°F)
Sequential heating,
°C (°F)
Front-half catch
Particulate (ambient)
mg ,
mg/m
gr/dscf
Add soluble sulfate
as [H2S04(H20)2]
mg 3
mg/m
gr/dscf
Water soluble sulfate
as [S04=]
mg ,
mg/m
gr/dscf
Back-half catch
Sulfurlc acid mist
mg .
mg/m
gr/dscf
ppm
Sulfur dioxide
mg ,
mg/m
gr/dscf
ppm
Inorganic condensibles
mg 3
mg/m
gr/dscf
Organic condensibles
mg 3
mg/m
gr/dscf
Total organic carbon
mg 3
mg/m
gr/dscf
Test No.
06. 1
121
(250)
132
(270)
12.2
7.8
0.003
0.0
0.0
0.000
0.0
0.0
0.000
13.2
8.5
0.004
2
118.3
75.8
0.033
28
06.2
121
(250)
120
(248)
204
(400)
21.1
13.5
0.006
0.0
0.0
0.000
0.0
0.0
0.000
55.2
35.4
0.015
2.4
1.5
0.0007
403a
258
0.113
D6.3
204
(400)
204
(399)
15.6
10.8
0.005
1.4
1.0
0.0004
0.0
0.0
0.000
7.5
5.2
0.002
1
113.3
78.1
0.034
29
06. 4
204
(400)
219
(427)
12.0
8.0
0.004
0.0
0.0
0.000
0.0
0.0
0.000
144.2
96.8
0.042
2.8
1.9
0.0008
77a
51.7
0.022
D6.5
121
(250)
131
(267)
316
(600)
19.9
10.9
0.005
0.0
0.0
0.000
0.0
0.0
0.000
10.0
5.5
0.002
2.4
1.3
0.0006
8.0
4.4
0.002
06. 6
316
(600)
319
(607)
9.2
6.3
0.003
0.3
0.2
0.0001
0.0
0.0
0.000
11.4
7.9
0,003
2
110.1
75.9
0.033
28
Contaminated with isopropanol.
2-24
-------
No water soluble sulfates were found on NCOG filters and acetone
rinse residues. Figures 2-1 and 2-2 present graphs plotting
particulate concentration versus average filter temperature for
NCOG and DCOG underfiring, respectively. A line of best fit was
determined for each data set by a least-squares linear regression
calculation. Performance of this calculation, showed that the
NCOG data more accurately depicted a bimodal line of best fit.
Figure 2-3 presents the NCOG and DCOG best fit lines for partic-
ulate concentration versus average filter temperature.
Analytical results obtained from Sampling Trains 1 and 2
[121°C (250°F) front-half temperature], Sampling Trains 3 and 4
[177°C (350°F) or 204°C (400°F) front-half temperature], Sampling
Train 5 [121°C (250°F) front-half temperature], and Sampling
Train 6 [316°C (600°F) front-half temperature] are presented in
Tables 2-20, 2-21, 2-22, and 2-23 for the NCOG underfiring test
series and Tables 2-24, 2-25, 2-26, and 2-27 for the DCOG under-
firing test series, respectively.
Visible emissions observations and process data collected
during particulate testing are presented in Sections 2.5 and 2-10
of this report.
2-25
-------
160
140
120
f> 100
z
o
h-
-------
40
<_)
§
30
I
RUN 1
RUN 2
RUN 3
RUN 4
RUN 5
RUN 6
LINE OF BEST FIT
V INT • 23.8
SLOPE - -0.031
CORR. COEF. - -0.254
cc.
a.
a.
20
10
O a
O
O
100 200
AVERAGE ACTUAL FILTER TEMPERATURE, *C
300
Figure 2-2. Particulate concentration vs. average actual
filter temperature during DCOG underfiring.
2-27
-------
S
o
LJ
160
140
120
100
no
60
oc
KC
o.
40
20
NCOG, B
NCOG, A
DCOG
1
100 200
AVERAGE ACTUAL FILTER TEMPERATURE, °C
300
Figure 2-3. Summary of best-fit lines from particulate concentration
vs. average actual filter temperature for NCOG and DCOG underfiring.
2-28
-------
TABLE 2-20. NCOG UNDERFIRING CONDITION, TRAINS 1 AND 2 OF QUAD TRAIN
[121°C (250°F) FRONT HALF]
NJ
VO
Date (1981)
Actual average filter
temperature. °C (°F)
Sequential heating (2 hours),
°C (°r)
Front-half catch
Participate (ambient)
mq ,
mg/m
qr/dscf
» loss
Acid soluble sulfate
as [H;S04]
mq ,
mg/m
gr/dscf
as [H2S04(HZ0)2]
mg ,
mg/m
gr/dscf
Back-half catch
Sulfurlc add mist
mg 3
mg/mj
gr/dscf
Sulfur dioxide
mq
mg/m
ar/dscf
Ppm
Inorganic condenslbles
mg -
mq/mj
gr/dscf
Organic condenslbles
mg -
mg/m
gr/dscf
Total organic carbon
mg ..
mq/mj
gr/dscf
1.1
10/27
122
(252)
226.9
128.9
0.056
81.5
46.3
0.020
111.4
63.3
0.028
8.9
5.0
0.002
1960
1114
0.486
419
-
-
-
1.2
10/27
125
(257)
Amb.
192.8
115.4
0.050
-
-
177
(350)
55.2
33.0
0.014
72
7.4
4.4
0.002
10.1
6.1
0.003
9.4
5.6
0.002
1850
1108
0.4B4
416
-
-
-
3.1
10/28
113
(236)
202.0
115.4
0.050
70.4
40.2
0.017
96.2
55.0
0.024
3.3
4.7
0.002
1790
1023
0.446
384
-
-
-
Test No.
3.2
10/28
127
(260)
Amb.
156.9
94.5
0.041
-
-
177
(350)
34.2
20.6
0.009
78
0.0
0.0
0.000
0.0
0.0
0.000
8.6
5.2
0.002
1540
928
0.406
349
-
-
-
5.1
10/29
124
(255)
138.6
84.5
0.037
85.6
52.2
0.023
117.0
71.3
0.031
34.4
21.0
D.009
2070
1262
0.550
474
-
-
-
5.2
10/29
123
(254)
Amb.
185.6
123.7
0.054
-
-
177
(350)
36.8
24.5
0.011
80
3.0
2.0
0.0008
4.1
2.7
0.004
-
-
19.0
12.7
0.006
4.2
2.8
0.001
58.1
38.7
0.017
2.1
10/27
119
(247)
183.1
115.2
0.050
61.6
38.7
0.017
84.2
53.0
0.023
741a
466
0.204
1370
862
0.377
324
-
-
-
2.2
10/27
128
(263)
Amb.
149.2
99.5
0.044
-
-
204
(400)
24.8
16.5
0.007
84
0.0
0.0
0.000
0.0
0.0
0.000
16.0
10.7
0.005
1720
1147
0.502
431
-
-
-
4.1
10/28
123
(254)
139.9
141.3
0.062
47.5
47.9
0.021
64.9
65.6
0.029
11.5
11.6
0.005
1300
1313
0.577
494
-
-
-
4.2
10/28
130
(266)
Amb.
113.2
128.6
0.056
-
-
204
(400)
41.7
47.4
0.021
62
0.4
0.4
0.0002
0.5
0.6
0.0002
11.9
13.5
0.006
1170
1329
0.58)
500
-
-
-
6.1
10/29
119
(246)
184.1
112.2
0.049
71.0
43.3
0.019
97.0
59.6
0.026
24.0
14.6
0.006
2000
1219
0.532
458
-
-
-
6.2
10/29
126
(258)
Amb.
150.8
97.9
0.043
-
-
204
(400)
24.2
15.7
0.007
84
0.0
0.0
0.000
0.0
0.0
0.000
-
-
109.7
71.2
0.031
4.0
2.6
0.001
42.3
27.5
0.012
-------
TABLE 2-21. NCOG UNDERFIRING CONDITION, TRAINS 3 AND 4 OF QUAD TRAIN
[1*1°C (250°F) AND 204°C (400°F) FRONT HALF]
Test No.
Date (1981)
Actual average filter
temperature, °C (°F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04]
mg -
mg/m
gr/dscf
as [H2SO,j(H20)2]
mq -
mg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mo ,
mg/m
gr/dscf
Sulfur dioxide
mg ,
mg/mj
gr/dscf
ppm
Inorganic condensibles
mg »
mg/m
gr/dscf
Organic condensibles
mg 3
mg/m
gr/dscf
Total organic carbon
mg carbon
mg/m3
gr/dscf
1.3
10/27
170
(338)
72.9
43.4
0.019
9.8
5.8
0.002
13.4
8.0
0.003
65.4
38.9
0.017
1870
1113
0.487
418
-
-
-
1.4
10/27
169
(336)
50.6
30.8
0.013
4.7
2.9
0.001
6.4
3.9
0.002
56.0
34.1
0.015
1810
1104
0.482
415
-
-
-
we
3.3
10/28
178
(353)
87.3
53.6
0.023
25.3
15.5
0.007
34.6
21.2
0.009
67.2
41.2
0.018
1680
1031
0.450
387
-
-
-
(350°F)
3.4
10/28
169
(336)
40.3
25.5
0.011
3.7
2.3
0.001
5.0
1.2
0.001
89.2
56.4
0.025
1620
1025
0.448
385
-
-
-
5.3
10/29
176
(349)
50.5
33.0
0.014
9.5
6.2
0.003
13.0
8.5
0.004
81.5
53.3
0.023
1970
1288
0.564
484
-
-
-
5.4
10/29
186
(366)
32.1
22.4
0.010
0.0
0.0
0.000
0.0
0.0
0.000
-
-
101.2
70.8
0.031
3.2
2.2
0.001
49.2
34.4
0.015
2.3
10/27
198
(389)
46.3
31.7
0.014
12.2
3.3
0.004
16.7
11.4
0.005
53.0
36.3
0.016
1700
1164
0.509
438
-
-
-
2.4
10/27
207
(404)
61.3
42.6
0.019
14.4
10.0
0.004
19.7
13.7
0.006
19.6
13.6
0.006
1610
1118
0.489
420
-
-
-
204 «C
4.3
10/28
177
(350)
61.1
65.7
0.028
6.4
6.9
0.003
8.7
9.4
0.004
29.8
32.0
0.014
1250
1344
0.585
505
-
-
(400-F)
4.4
10/28
169
(337)
78. 4
92.2
0.040
12.6
14.8
0.006
17.2
20.3
0.009
10.4
12.2
0.005
1160
1365
0.596
513
-
-
-
6.3
10/29
193
(379)
34.3
22.6
0.010
2.8 .
1.8
0.0008
3.8
2.5
o!ooi
97.6
64.2
0.028
1900
1250
0.546
470
-
-
-
6.4
10/29
208
(407)
26.9
20.8
0.009
0.0
0.0
0.000
0.0
0.0
0.000
-
118.3
91.7
0.040
5.9
4.6
0.002
154a
119.4
0.052
Isopropanol contaminated.
2-30
-------
TABLE 2-22. NCOG UNDERFIRING CONDITION, TRAIN 5
[121°C (250°F) FRONT HALF]
to
I
U)
Actual average filter
temperature, °C (°F)
Front-half catch
Filter half designa-
tion
Sequential heating,
°C (°F)
Heating time, h
Particulate (ambient)
mg 3
mg/m
gr/dscf h
J difference
Acid sul fates
Total organic carbon
Back-half catch
Inorganic condenslbles
mg -
mg/m
gr/dscf
Organic condenslbles
mg -
mg/m
gr/dscf
Total organic carbon
mg carbon
mq/m3
gr/dscf
Test No. 1.5 (10/27/81)
128 (263)
A
177 177 204
Antb. (350) (350) (400)
242
135.3 47.5 41.7 37.3
94.0 33.0 29.0 25.9
0.041 0.014 0.013 0.011
66 68 73
204
(400)
4
34.5
24.0
0.010
76
316
(600)
2
30.5
21.2
0.009
78
NOC
B
NO
28.2
19.6
0.008
2.6
1.8
0.001
23.4
16.2
0.007
Test Ho. 2.5 (10/27/81)
125 (257)
A
177 177 204 204
An*. (350) (350) (400) (400)
2424
90.9 34.0 30.7 29.2 27.7
60.6 22.7 20.5 19.5 18.5
0.026 0.010 0.009 0.008 0.008
62 62 69 69
316
(600)
2
22.5
15.0
0.006
77
ND
B
NO
68.2
45.5
0.020
4.8
3.2
0.001
44.3
29.5
0.013
-------
TABLE 2-22 (continued)
Actual average filter
temperature, "C (°F)
Front-half catch
Filter half designa-
tion
Sequential heating,
°C (°F)
Heating time, h
Participate (ambient)
mg ,
mg/m
gr/dscf
% differenceb
Add sulfates
Total organic carbon
Back-half catch
Inorganic condenslbles
mg -
mg/m
flr/dscf
Organic condenslbles
mfl 3
mg/m
gr/dscf
Total organic carbon
mg carbon
mg/m3
gr/dscf
Test No. 3.5 (10/28/81)
109 (229)
A
177 177 204
Amb. (350) (350) (400)
242
171.2 29.0 26.8 26.2
99.5 16.9 15.6 15.2
0.043 0.007 0.007 0.007
84 84 84
204
(400)
4
25.2
14.6
0.006
86
316
(600)
2
22.0
12.8
0.006
86
NO
B
ND
99.1
57.6
0.025
3.2
1.9
0.001
77.3
44.9
0.020
Test No. 4.5 (10/28/81)
130 (266)
A
177 177 204 204 316
Amb. (350) (350) (400) (400) (600)
24242
174.5 137.3 128.8 112.4 104.7 99.0
80.0 63.0 59.1 51.6 48.0 45.4
0.035 0.028 0.026 0.022 0.021 0.020
20 26 37 40 43
ND
B
ND
65.7
30.1
0.0!3
3.1
1.4
0.001
14.3
6.6
0.003
to
I
u>
-------
TABLE 2-22 (continued)
to
I
w
u>
Actual average filter
temperature, °C (°F)
Front-half catch
Filter half designa-
tion
Sequential heating,
°C (°F)
Heating time, h
Partlculate (ambient)
mg 3
mg/m
gr/dscf .
% difference"
Acid sul fates
Total organic carbon
Back-half catch
Inorganic condenslbles
mV
gr/dscf
Organic condenslbles
mg 3
mg/m
gr/dscf
Total organic carbon
mg carbon
mg/nK
gr/dscf
Test Mo. 5.5 (10/29/81)
116 (240)
A
177 177 204 204 316
Amb. (350) (350) (400) (400) (600)
24242
221.0 50.4 44.2 36.2 32.3 27.7
137.3 31.3 27.4 22.5 20.1 17.2
0.060 0.014 0.012 0.010 0.009 0.008
77 80 83 85 87
NO
B
NO
20.9
13.0
0.006
6.3
3.9
0.002
11.8
7.3
0.003
Test No. 6.5 (10/29/81)
119 (246)
A
177 177 204 204 316
Amb. (350) (350) (400) (400) (600)
24242
195.7 42.3 37.6 33.2 30.3 25.8
118.6 25.6 22.8 20.1 18.4 15.6
0.052 0.011 0.010 0.009 0.008 0.007
79 81 83 85 86
NO
B
NO
20.0
12.1
0.005
6.4
3.9
0.002
15.2
9.2
0.004
"All weights corrected to entire filter catch.
Calculated from concentration.
CND - Not detectable, sample response egualed blank response.
-------
TABLE 2-23. NCOG UNDERFIRING CONDITION, TRAIN 6
[316°C (600°F) FRONT HALF]
Date (1981)
Actual average filter
temperature, °C (°F)
Front-half catch
Particulate (ambient)
mg 3
mg/m
gr/dscf
Acid soluble sulfate
as [H2S04]
mg 3
mg/m
gr/dscf
as [H2S04(H20)2]
mg 3
mg/m
gr/dscf
Back-half catch
Sulfuric acid mist
mg 3
mg/m
gr/dscf
Sulfur dioxide
mg 3
mg/m
gr/dscf
Ppm
Test No.
1.6
10/27
320
(608)
27.0
19.0
0.008
0.0
0.0
0.000
0.0
0.0
0.000
606a
426.8
0.187
1120
789
0.346
296
2.6
10/27
316
(600)
39.5
23.9
0.010
2.6
1.6
0.001
3.5
2.1
0.001
157
95.7
0.041
1940
1176
0.512
442
3.6
10/28
293
(560)
36.0
19.6
0.008
4.2
2.3
0.001
5.7
3.1
0.001
164
89.1
0.039
1720
935
0.408
351
4.6
10/28
328
(622)
69.7
62.8
0.027
0.0
0.0
0.000
0.0
0.0
0.000
73.7
66.4
0.029
1550
1396
0.611
525
5.6
10/29
324
(616)
24.9
16.2
0.007
0.0
0.0
0.000
0.0
0.0
0.000
129
83.8
0.036
2050
1331
0.581
500
6.6
10/29
302
(576)
30.9
19.6
0.008
0.0
0.0
0.000
0.0
0.0
0.000
115
72.8
0.032
2010
1272
0.555
478
Hydrogen peroxide contaminated.
2-34
-------
TABLE 2-24. DCOG UNDERFIRING CONDITION, TRAINS 1 AND 2 OF QUAD TRAIN
[121°C (250°F) FRONT HALF]
Date (1981)
Actual average filter
temperature. °C (°F)
Sequential heating (2 hours),
°C (°F)
Front-half catch
Partlculate (ambient)
mg ,
mg/m
gr/dscf
X loss
Acid soluble sulfate
as [H2S04(HZ0)2]
mg ,
mg/m
gr/dscf
Hater soluble sulfate
as [S04=]
mg
mg/m3
gr/dscf
Back-half catch
SulfuHc add mist
mg ,
mg/mj
gr/dscf
Sulfur dioxide
mg ,
mg/m
gr/dstf
ppm
Inorganic condensibles
mg -
mg/m
gr/dscf
Organic condensibles
mg 3
mg/m
gr/dscf
Total organic carbon
mg carbon
mg/nr
gr/dscf
Test Ho.
01.1
12/8
119
(246)
316
(600)
32.6
26.1
0.011
0.0
0.0
0.000
<0.3
0.2
-0.004
115b
92
0.040
69.7
55.8
0.024
21
-
-
-
01. 2
12/8
133
(272)
Anb.
37.4
33.4
0.014
-
-
177
(350)
22.0
19.6
0.008
41
2.7
2.4
0.001
2.1
1.9
0.001
3.5
3.1
0.001
116.1
103.7
0.045
39
-
-
-
D2.1
12/10
118
(244)
249.9
178.5
0.078
1.4
1.0
0.0004
0.9
0.6
0.0003
13.7
9.8
0.004
120.8
86.3
0.038
32
-
-
-
D2.2
12/10
109
(229)
Arab.
38.3
21.5
0.009
-
-
177
(350)
24.6
13.8
0.006
36
3.5
2.0
0.001
2.0
1.1
0.001
14.4
8.1
0.004
159.4
89.6
0.039
34
-
-
-
05.1
12/12
123
(253)
23.3
13.4
0.006
4.6
2.6
0.001
3.7
2.1
0.001
8.8
5.0
0.002
31.8
75.7
D.033
28
-
-
-
05. 2
12/12
127
(261)
An*.
20.0
11.5
0.005
-
-
177
(350)
8.7
5.0
0.002
56
1.1
0.6
0.0003
1.7
1.0
0.001
-
-
74.5
42.8
0.019
0.70
0.40
0.0002
202C
116
0.050
03.1 '
12/11
120
(248)
38.6
26.1
0.011
0.4
0.3
0.000
6.0
4.0
0.002
84. Ob
56.8
0.025
90.1
60.9
0.026
23
-
-
-
03. 2
12/11
132
(270)
Amb.
34.5
21.3
0.009
-
204
(400)
18.1
11.2
0.005
47
2.5
1.5
0.001
0.0
0.0
O.OOC
7.0
4.3
0.002
152.8
94.3
0.041
35
-
-
-
04.1
12/12
148
(299)
28.5
16.9
0.007
0.0
0.0
0.000
0.0
0.0
0.000
42.3b
25.0
0.011
35.6
80.2
D.035
30
-
-
-
04.2
12/12
126
(259)
Amb.
45.2
26.7
0.012
-
-
204
(400)
13.5
8.0
0.003
70
0.0
0.0
0.001
0.9
0.5
0.0002
15.9
9.4
0.004
130.5
77.2
0.034
30
-
-
-
06.1
12/13
132
;270)
12.2
7.8
0.003
0.0
0.0
0.000
0.0
0.0
0.000
13.2
8.5
0.004
118.3
75.8
1.033
28
-
-
-
06. 2
12/13
120
(248)
Ainb.
21.1
13.5
0.006
-
-
204
(400)
5.4
3.5
0.001
74
0.0
0.0
0.000
0.0
0.0
0.000
-
-
55.2
35.4
0.015
2.4
1.5
0.0007
403C
258
0.113
NJ
I
Ul
cn
aAcetone rinse contaminated with oil.
Hydrogen peroxide contaminated.
clsopropanol contaminated.
-------
TABLE 2-25.
DCOG UNDERFIRING CONDITION, TRAINS 3 AND 4 OF QUAD TRAIN
[177°C (350°F) AND 204°C (400°F) FRONT HALF]
Test No.
Date (1981)
Actual average filter
temperature. °C (°F)
Front-half catch
Participate (ambient)
mg 3
mg/m
gr/dscf
Add soluble sulfate
as [H2S04(HzO)2]
mg ,
mg/m
gr/dscf
Hater soluble sulfate
as [S04=]
mg 3
mg/m
gr/dscf
Back-half catch
Sulfurlc add mist
mg ,
mg/m
gr/dscf
Sulfur dioxide
mg ,
mg/m
gr/dscf
ppm
Inorganic condensibles
mg ,
mg/m
gr/dscf
Organic condensibles
mg 3
mg/m
gr/dscf
Total organic carbon
mg carbon
mg/m3
gr/dscf
177°C (350"F)
01.3
12/8
190 (374)
34.0
29.3
0.013
0.0
0.0
0.000
2.5
2.1
0.001
9.3
8.0
0.004
117.0
100.9
0.044
38
-
-
-
01.4
12/8
167 (333)
43.3
38.7
0.017
0.0
0.0
0.000
0.0
0.0
0.000
9.2
8.2
0.004
115.8
113.4
0.045
39
-
-
-
02. 3
12/10
184 (363)
34.8
20.4
0.009
0.8
0.5
0.0001
3.5
2.0
0.001
8.7
5.1
0.002
155.0
90.6
0.040
34
-
-
-
02.4
12/10
197 (387)
37.2
20.8
0.009
0.5
0.3
0.0001
4.8
2.7
0.002
54. 8a
30.6
0.013
131.8
73.6
0.032
28
-
-
-
05.3
12/12
181 (357)
16.3
10.4
0.004
3.0
1.9
0.001
1.6
1.0
0.0004
7.8
5.0
0.002
123.6
79.2
0.035
30
-
- •
-
05.4
12/12
177 (351)
19.1
11.9
0.005
0.8
0.5
0.0002
3.8
2.4
0.001
-
-
158.1
98.8
0.043
4.0
2.5
0.001
572b
357
0.156
204'C (400"F)
03.3
12/11
211 (411)
30.9
22.1
0.010
0.0
0.0
0.000
4.1
2.9
0.002
12.0
8.6
0.004
130.8
93.4
0.041
35
-
-
-
03.4
12/11
204 (400)
38.7
26.9
0.012
2.6
1.8
0.001
0.8
0.5
0.0003
8.2
5.7
0.002
143.4
99.6
0.043
37
-
-
-
04.3
12/12
209 (409)
24.8
16.6
0.007
0.9
0.6
0.0003
3.2
2.1
0.001
6.7
4.5
0.002
118.3
79.4
0.035
30
-
-
-
04.4
Void
run
06.3
12/13
204 (399)
15.6
10.8
0.005
1.4
1.0
0.0004
0.0
0.0
0.000
7.5
5.2
0.002
113.3
78.1
0.034
29
-
-
-
D6.4
12/13
219 (427)
12.0
8.0
0.004
0.0
0.0
0.000
0.0
0.0
0.000
-
-
144.2
96.8
0.042
2.8
1.9
0.0008
77b
51.7
0.022
to
I
'Hydrogen peroxide contaminated.
Isopropanol contaminated.
-------
TABLE 2-26. DCOG UNDERFIRING CONDITION, TRAIN
[121°C (250°F) FRONT HALF]
Actual average filter
temperature, "C (°F)
Front-half catch
Filter half designa-
tion
Sequential heating,
•C (°F)
Heating time, h
Partlculate (ambient)
mg 3
mg/m
gr/dscf h
* difference"
Add sul fates
as [H2S04(H20)2]
mq ,
mg/m
gr/dscf
Water soluble sulfate
as [S04=]
mg -
mg/m
gr/dscf
Total organic carbon
Back-half catch
Inorganic condenslbles
mg 3
mg/m
gr/dscf
Organic condenslbles
mg ,
mg/m
gr/dscf
Total organic carbon
mg carbon
mg/m3
gr/dscf
Test No. 01. 1 (12/8/81)
119 (246)
A
177 177 204 204 316
Afflb. (350) (350) (400) (400) (600)
24242
32.6 21.8 21.1 16.8 16.4 14.6
26.1 17.4 16.9 13.4 13.1 11.7
0.011 0.008 0.007 0.006 0.006 0.005
33 35 49 50 55
0.0
0.0
0.000
<0.3
<0.2
<0.0001
B
NOC
N/Ad
N/A
N/A
Test No. 02.5 (12/10/81)
126 (258)
A
177 177 204 204 316
Amb. (350) (350) (400) (400) (600)
24242
41.1 23.4 19.2 18.8 17.7 15.1
22.3 12.7 10.4 10.2 9.6 8.2
0.010 0.005 0.004 0.004 0.004 0.003
43 53 54 57 63
0.0
0.0
0.000
0.0
0.0
0.000
B
NO
152.6
82.9
0.036
0.8
0.4
0.0002
8.6
4.7
0.002
to
I
OJ
-------
TABLE 2-26 (continued)
Actual average filter
temperature, °C (°F)
Front-half catch
Filter half designa-
tion
Sequential heating,
°C (°F)
Heating time, h
Participate (ambient)
ng .
mg/m
gr/dscf h
I difference
Acid sui fates
as [H2SOA(H20)2]
mg 3
mg/m
gr/dscf
Water soluble sui fate
»s tSQ4=]
mq ,
mg/m'
gr/dscf
Total organic carbon
Back-half catch
Inorganic condenslbles
mg ,
mg/m
gr/dscf
Organic condenslbles
mg j
mg/m
gr/dscf
Total organic carbon
mg carbon
mg/m'
gr/dscf
Test No.
D3.5 (12/11/81)
123 (254)
A
177 177
Amb. (350) (350)
2 4
35.0 22.2 19.9
19.6 12.4 11.1
0.008 0.005 0.005
37 43
0.
0.
0.
204 204 316
(400) (400) (600)
242
15.7 15.7 13.4
8.8 8.8 7.5
0.004 0.004 0.003
55 55 62
0
0
000
0.9
0.5
0.0002
B
ND
28.9
16.1
0.007
2.0
1.1
0.0005
3.4
1.9
0.0008
Vest No.
D4.5 (12/12/81)
128 (263)
A
177 177
Amb. (350) (350)
2 4
31.2 21.7 20.2
17.8 12.4 11.5
0.008 0.005 0.005
34 35
0.
0.
0.
0.
0.
0.
204 204 316
(400) (400) (600)
242
15.1 14.9 12.3
8.6 8.5 7.0
0.004 0.004 0.005
52 52 61
0
0
000
0
0
000
84
48
0.
B
HD
.5
.3
021
2.9
1.6
0.0007
8.5
4.8
0.002
I
to
00
-------
TABLE 2-26 (continued)
Actual average filter
temperature, °C (°F)
Front-half catch
Filter half designa-
tion
Sequential heating.
°C (°F)
Heating time, h
Paniculate (ambient)
m", 3
mg/m
gr/dscf .
% difference0
Acid sul fates
as [H2S04(H20)2]
mg 3
mg/m
gr/dscf
Hater soluble sulfate
as [S04~]
mg ,
mg/m
gr/dscf
Total organic carbon
Back-half catch
Inorganic condensibles
mg ,
mg/m
gr/dscf
Organic condensibles
mg ,
mg/m
gr/dscf
Total organic carbon
mg carbon
mq/m3
gr/dscf
Test No
05. 5 (12/12/81)
122 (251)
A
177 177
Amb. (350) (350)
2 4
1S.9 6.9 5.3
9.4 4.1 3.1
0.004 0.002 0.001
56 67
0.
0.
0.
0.
0.
0.
204 204 316
(400) (400) (600)
242
4.5 4.5 2.4
2.7 2.7 1.4
0.001 0.001 0.001
71 71 85
0
0
000
0
0
0002
B
NO
15.6
9.2
0.004
1.
0.
0.
3.
2.
0.
4
8
0004
6
0009
Test No.
06.5 (12/13/81)
131 (267)
A
177 177
Amb. (350) (350)
2 4
19.9 13.6 12.8
10.9 7.4 7.0
0.005 0.003 0.003
32 26
204 204 316
(400) (400) (600)
242
11.5 11.3 4.4
6.3 6.2 2.4
0.003 0.003 0.001
42 43 78
0.0
0.0
0.000
0.
0.
0.
0
0
000
B
NO
. 10.0
5.5
0.002
2.4
1.3
0.0006
8.0
4.4
0.002
to
I
co
vo
aA11 weights corrected to entire filter catch.
Calculated from concentration.
NO = Not detectable, sample response similar to blank response.
dN/A = Not analyzed.
-------
TABLE 2-27. DCOG UNDERFIRING CONDITION, TRAIN 6
[316°C (600°F) FRONT HALF]
Date (1981)
Actual average filter
temperature, °C (°F)
Front-half catch
Particulate (ambient)
mg ,
mg/tn
gr/dscf
Acid soluble sulfate
as [H2S04(H20)2]
mg ,
mg/'m
gr/dscf
Water soluble sulfate
as [S0
-------
2.3 COMPARISON OF PARTICULATE RESULTS AT SELECTED TEMPERATURES
Selected particulate samples collected at a probe and filter
temperature of approximately 121°C (250°F) were sequentially
heated to determine weight loss at 177°C (350°F), 204°C (400°F),
and 316°C (600°F). Tables 2-28 and 2-29 present the results from
the sequential heating of the NCOG and DCOG samples, respec-
tively. This data showed that more than half of the weight loss
occurred when the sample was initially heated to 177°C (350°F).
Therefore, a sample was sequentially heated in 14°C (25°F) incre-
ments to determine at what temperature the highest weight loss
occurred. This data is presented in Table 2-30. Figures 2-4 and
2-5 present this data graphically.
Tables 2-31 through 2-33 present data comparing particulate
concentrations determined from sampling at two different tempera-
tures [177°C (350°F) versus 121°C (250°F), but analyzing after
heat treatment at 177°C (350°F); 204°C (400°F) versus 121°C
(250°F), but analyzed after heat treatment at 204°C (400°F); and
316°C (600°F) versus 121°C (250°F) but analyzing after treatment
at 316°C (600°F)] for NCOG underfiring. Tables 2-34 through 2-36
present these data for DCOG underfiring.
2-41
-------
TABLE 2-28. RESULTS OF SEQUENTIAL HEATING OF SELECTED NCOG
UNDERFIRING TEST SERIES SAMPLES
Sequential
heating
Temperature,
°C («F)
Time,
h
Participate weight
Front-half Hnse
mg
% weight
loss
Filter
mg
X weight
loss
Total
mg
I weight
loss
Sampling Train 1.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
_
2
4
2
4
2
82.3
26.1
21.6
17.8
15.6
12.5
.
68
74
78
81
85
53.0
21.4
20.1
19.5
18.9
18.0
_
60
62
63
64
66
135.3
47.5
41.7
37.3
34.5
30.5
^
65
69
72
74
77
Sampling Train 2.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
•
2
4
2
4
2
62.8
18.4
15.5
14.4
13.3
10.3
.
71
75
77
79
83
28.1
15.6
15.2
14.8
14.4
12.2
_
44
46
47
49
56
90.9
34.0
30.7
29.2
27.7
22.5
»
63
66
68
69
75
Sampling Train 3.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
_
2
4
2
4
2
74.5
10.6
8.6
8.4
7.8
5.6
_
86
88
89
89
92
96.7
18.4
18.2
17.8
17.4
16.4
_
81
81
82
82
83
171.2
29.0
26.8
26.2
25.2
22.0
•
83
84
85
85
87
Sampling Train 4.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
_
2
4
2
4
2
59.8
34.8
29.8
22.4
16.8
14.0
.
42
50
62
72
77
114.7
102.5
99.0
90.0
87.9
85.0
.
11
14
21
23
26
174.5
137.3
128.8
112.4
104.7
99.0
w
21
26
35
40
43
Sampling Train 5.5
Ambient
177 (350
177 (350
204 (400
204 (400
316 600
.
2
4
2
4
2
117.0
27.6
24.7
17.9
17.4
10.9
_
76
79
85
87
91
103.2
22.8
19.5
18.3
17.6
16.8
.
78
81
82
83
84
221.0
50.4
44.2
36.2
32.3
27.7
^
77
80
84
85
87
Sampling Train 6.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
—
2
4
2
4
2
108.1
28.6
25.9
21.9
19.8
16.5
.
73
76
80
82
85
87.6
13.7
11.7
11.3
10.5
9.3
.
84
87
87
88
89
195.7
42.3
37.6
33.2
30.3
25.8
_
78
81
83
84
87
2-42
-------
TABLE 2-29. RESULTS OF SEQUENTIAL HEATING OF SELECTED DCOG
UNDERFIRING TEST SERIES SAMPLES
Sequential
heating
Temperature,
•C (°F)
Time,
h
Participate weight
Front-hal? Hnse
mg
% weight
loss
Filter
mg
* weight
loss
Total
mg
% weight
loss
Sampling Train D1.5
Ambient
177
177
204
350)
350)
400)
204 (400)
316 (600)
—
2
4
2
4
2
18.0
B.4
7.9
5.4
5.4
3.8
m
53
56
70
70
79
14.6
13.4
13.2
11.4
11.0
10.8
m
8
9
22
25
26
32.6
21.8
21.1
16.8
16.4
14.6
—
33
35
48
50
55
Sampling Train 02.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
.
2
4
2
4
2
24.4
11.0
9.3
8.9
8.0
6.2
.
55
62
63
67
74
16.7
12.4
9.9
9.9
9.7
6.9
.
26
41
41
42
47
41.1
23.4
19.2
18.8
17.7
15.1
.
43
53
54
57
63
Sampling Train D3.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
.
2
4
2
4
2
18.9
7.3
6.0
5.3
5.3
4.2
_
61
68
72
72
78
16.1
14.9
13.9
10.4
10.4
9.2
_
7
14
35
35
43
35.0
22.2
19.9
15.7
15.7
13.4
—
36
43
55
55
62
Sampling Train 04.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
_
2
4
2
4
2
19.6
13.4
13.1
7.6
7.6
6.0
_
32
33
61
61
69
11.6
8.3
7.1
7.5
7.3
6.3
_
28
39
35
37
46
31.2
21.7
20.2
15.1
14.9
12.3
.
30
35
52
52
60
Sampling Train 05.5
Ambient
177
177
204
204
350)
350)
400)
400)
316 (600)
_
2
4
2
4
2
9.5
2.6
2.5
2.5
2.5
1.4
_
72
74
74
74
85
6.4
4.3
2.8
2.0
2.0
1.0
_
33
56
69
69
84
15.9
6.9
5,3
4.5
4.5
2.4
_
57
67
72
72
85
Sampling Train 06.5
Ambient
177 (350)
177 (350)
204 (400)
204 (400)
316 (600)
_
2
4
2
4
2
12.6
8.4
7.8
6.5
6.5
1.0
.
33
38
48
48
92
7.3
5.2
5.0
5.0
4.8
3.4
.
29
31
31
34
53
19.9
13.6
12.8
11.5
11.3
4.4
.
32
36
42
43
78
2-43
-------
TABLE 2-30. RESULTS OF SEQUENTIAL HEATING OF
SELECTED NCOG UNDERFIRING TEST SERIES RUN 8.5, FRONT HALF
Sequential
heating
Temperature,
°C (°F)
Ambient
135 (275)
149 (300)
163 (325)
177 (350)
204 (400)
316 (600)
Time,
h
-
2
4
2
4
2
4
2
4
2
4
2
Particulate weight
Front-half rinse
mg
85.4
32.3
23.9
22.1
20.1
18.7
17.6
15.7
15.3
11.3
10.0
6.4
% weight
loss
-
62
72
74
76
78
79
82
82
87
88
92
Filter
mg
98.5
43.2
42.8
42.4
42.3
42.3
42.3
42.2
42.1
41.6
40.9
39.2
% weight
loss
-
56
56
57
57
57
57
57
57
58
58
60
Total
mg
183.9
75.5
66.7
64.5
62.4
61.0
59.9
57.9
57.4
52.9
50.9
45.6
% weight
loss
-
59
64
65
66
67
67
68
69
71
72
75
Source concentration
mg/m
129.5
53.2
47.0
45.4
43.9
43.0
42.2
40.8
40.4
37.2
35.8
32.1
gr/dscf
0.056
0.023
0.021
0.020
0.019
0.019
0.018
0.018
0.017
0.016
0.016
0.014
NJ
I
-------
100
I I I I I
I
•fc.
Ul
I/O
UJ
on
90
80
£ 70
60
RINSE
I I I I
0
135149163177 204
315
HEAT CONDITIONING TEMPERATURE, °C
Figure 2-4. Average percent weight loss from Sampling Train 5,
121°C (250°F) front-half temperature, due to heat conditioning
prior to weighing (MCOG underfiring).
-------
100
90
80
70
60
50
40
30
20
10
O
I
I
RINSE
177 204
HEAT CONDITIONING TEMPERATURE, *C
315
Figure 2-5. Average percent weight loss from Sampling Train 5,
121°C (250°F) front-half temperature, due to heat conditioning
prior to weighing (DCOG underfiring).
2-46
-------
"TABLE 2-31. COMPARISON OF PARTICIPATE CONCENTRATIONS DETERMINED
FROM SAMPLING AT TWO DIFFERENT TEMPERATURES UNDER NCOG UNDERFIRING
CONDITIONS: 177°C (350°F) VS. 121°C (250°F) BUT ANALYZING
AFTER TREATMENT AT 177°C (350°F)
Test No.
1.2
1.3
1.4
1.5
2.5
3.2
3.3
3.4
3.5
4.3
4.4
4.5
5.2
5.3
5.4
5.5
6.5
Date
(1981)
10/27
10/27
10/27
10/27
10/27
10/28
10/28
10/28
10/28
10/28
10/28
10/28
10/29
10/29
10/29
10/29
10/29
Actual filter
temperature,
°C (°F)
125 (257)
170 (338)
169 (336)
128 (263)
125 (257)
127 (260)
178 (353)
169 (336)
109 (229)
177 (350)
169 (337)
130 (266)
123 (254)
176 (349)
186 (366)
116 (240)
119 (246)
Sequential
heating
temperature,
°C (°F)
177 (350)
No
No
177 (350)
177 (350)
177 (350)
177 (350)
177 (350)
No
No
177 (350)
177 (350)
No
No
177 (350)
177 (350)
177 (350)
No
No
177 (350)
177 (350)
177 (350)
177 (350)
Heating
time, h
2
-
-
2
4
2
4
2
-
-
2
4
-
-
2
4
2
-
-
2
4
2
4
Front-half catch
particulate
mg
55.2
72.9
50.6
47.5
41.7
34.0
30.7
34.2
87.3
40.3
29.0
26.8
61.1
78.4
137.3
128.8
36.8
50.5
32.1
50.4
44.2
42.3
37.6
mg/m3
33.0
43.4
30.8
33.0
29.0
22.7
20.5
20.6
53.6
25.5
16.9
15.6
65.7
92.2
63.0
59.1
24.5
33.0
22.4
31.3
27.4
25.6
22.8
gr/dscf
0.014
0.019
0.013
0.014
0.013
0.010
0.009
0.009
0.023
0.011
0.007
0.007
0.028
0.040
0.028
0.026
0.011
0.014
0.010
0.014
0.012
0.011
0.010
2-47
-------
TABLE .2-32. COMPARISON OF PARTICULATE CONCENTRATIONS DETERMINED
FROM SAMPLING AT TWO DIFFERENT TEMPERATURES UNDER NCOG UNDERFIRING
CONDITIONS: 204°C (400°F) VS. 121 °C (250°F) BUT ANALYZING
AFTER TREATMENT AT 204°C (400°F)
Test No.
1.5
2.2
2.3
2.4
2.5
3.5
4.2
4.5
5.5
6.2
6.3
6.4
6.5
Date
(1981)
10/27
10/27
10/27
10/27
10/27
10/28
10/28
10/28
10/29
10/29
10/29
10/29
10/29
Actual filter
temperature,
°C (°F)
128 (263)
128 (263)
198 (389)
207 (404)
125 (257)
109 (229)
130 (266)
130 (266)
116 (240)
126 (258)
193 (379)
208 (407)
119 (246)
Sequential
heating
temperature,
°C (°F)
204 (400)
204 (400)
204 (400)
No
No
204 (400)
204 (400)
204 (400)
204 (400)
204 (400)
204 (400)
204 (400)
204 (400)
204 (400)
204 (400)
No
No
204 (400)
204 (400)
Heating
time, h
2
4
2
-
-
2
4
2
4
2
2
4
2
4
2
-
-
2
4
Front-half catch
particulate
mg
37.3
34.5
24.8
46.3
61.3
29.2
27.7
26.2
25.2
41.7
112.4
104.7
36.2
32.3
24.2
34.3
26.9
33.2
30.3
mg/m3
25.9
24.0
16.5
31.7
42.6
19.5
18.5
15.2
14.6
47.4
51.6
48.0
22.5
20.1
15.7
22.6
20.8
20.1
18.4
gr/dscf
0.011
0.010
0.007
0.014
0.019
0.008
0.008
0.007
0.006
0.021
0.022
0.021
0.010
0.009
0.007
0.010
0.009
0.009
0.008
2-48
-------
TABLE 2-33. COMPARISON OF PARTICULATE CONCENTRATIONS DETERMINED
FROM SAMPLING AT TWO DIFFERENT TEMPERATURES UNDER NCOG UNDERFIRING
CONDITIONS: 316°C (600°F) VS. 121°C (250°F) BUT ANALYZING
AFTER TREATMENT AT 315°C (600°F)
Test No.
1.5
1.6
2.5
2.6
3.5
3.6
4.5
4.6
5.5
5.6
6.5
6.6
Date
(1981)
10/27
10/27
10/27
10/27
10/28
10/28
10/28
10/28
10/29
10/29
10/29
10/29
Actual filter
temperature,
°C (°F)
128 (263)
320 (608)
125 (257)
316 (600)
109 (229)
293 (560)
130 (260)
328 (622)
116 (240)
324 (616)
119 (246)
302 (576)
Sequential
heating
temperature,
°C (°F)
316 (600)
No
316 (600)
No
316 (600)
No
316 (600)
No
316 (600)
No
316 (600)
No
Heating
time, h
2
-
2
-
2
-
2
-
2
-
2
-
Front-half catch
particulate
mg
30.5
27.0
22.5
39.5
22.0
36.0
99.0
69.7
27.7
24.9
25.8
30.9
mg/m3
21.2
19.0
15.0
23.9
12.8
19.6
45.4
62.8
17.2
16.2
15.6
19.6
gr/dscf
0.009
0.008
0.006
0.010
0.006
0.008
0.020
0.027
0.008
0.007
0.007
0.008
2-49
-------
TABLE 2-34. ,' COMPARISON OF PARTICULATE CONCENTRATIONS DETERMINED
FROM SAMPLING AT TWO DIFFERENT TEMPERATURES UNDER DCOG UNDERFIRING
CONDITIONS: 177°C (350°F) VS. 121°C (250°F) BUT ANALYZING
AFTER TREATMENT AT 177°C (350°F)
Test No.
Dl.l
D1.2
D1.3
D1.4
D2.2
D2.3
D2.4
D2.5
D3.5
D4.5
D5.2
D5.3
D5.4
D5.5
D6.5
Date
(1981)
12/8
12/8
12/8
12/8
12/10
12/10
12/10
12/10
12/11
12/12
12/12
12/12
12/12
12/12
12/13
Actual filter
temperature,
°C (°F)
119 (246)
133 (272)
190 (374)
167 (333)
109 (229)
184 (363)
197 (387)
126 (258)
123 (254)
128 (263)
127 (261)
181 (357)
177 (351)
122 (251)
131 (267)
Sequential
heating
temperature,
°C (°F)
177 (350)
177 (350)
-
-
177 (350)
-
-
177 (350)
177 (350)
177 (350)
177 (350)
-
-
177 (350)
177 (350)
Heating
time, h
2
4
2
-
-
2
-
-
2
4
2
4
2
4
2
-
-
2
4
2
4
Front-half catch
participate
mg
21 ;8
21.1
22.0
34.0
43.3
24.6
34.8
37.2
23.4
19.2
22.2
19.9
21.7
20.2
8.7
16.3
19.1
6.9
5.3
13.6
12.8
mg/mj
17.4
16.9
19.6
29.3
38.7
13.8
20.4
20.8
12.7
10.4
12.4
11.1
12.4
11.5
5.0
10.4
11.9
4.1
3.1
7.4
7.0
gr/dscf
0.008
0.007
0.008
0.013
0.017
0.006
0.009
0.009
0.005
0.004
0.005
0.005
0.005
0.005
0.002
0.004
0.005
0.002
0.001
0.003
0.003
2-50
-------
TABLE 2-35. COMPARISON OF PARTICULATE CONCENTRATIONS DETERMINED
FROM SAMPLING AT TWO DIFFERENT TEMPERATURES UNDER DCOG UNDERFIRING
CONDITIONS: 204°C (400°F) VS. 121°C (250°F) BUT ANALYZING
AFTER TREATMENT AT 204°C (400°F)
Test No.
Dl.l
D2.5
D3.2
D3.3
D3.4
D3.5
D4.2
D4.3
D4.5
D5.5
D6.2
D6.3
D6.4
D6.5
Date
(1981)
12/8
12/10
12/11
12/11
12/11
12/11
12/12
12/12
12/12
12/12
12/13
12/13
12/13
12/13
Actual filter
temperature,
°C (°F)
119 (246)
126 (258)
132 (270)
211 (411)
204 (400)
123 (254)
126 (259)
209 (409)
128 (263)
122 (251)
120 (248)
204 (399)
219 (427)
131 (267)
Sequential
heating
temperature,
°C (°F)
204 (400)
204 (400)
204 (400)
-
-
204 (400)
204 (400)
-
204 (400)
204 (400)
204 (400)
-
-
204 (400)
Heating
time, h
2
4
2
4
2
-
-
2
4
2
-
2
4
2
4
2
-
-
2
4
Front-half catch
particulate
mg
16.8
16.4
18.8
17.7
18.1
30.9
38.7
15.7
15.7
13.5
24.8
15.1
14.9
4.5
4.5
5.4
15.6
12.0
11.5
11.3
mg/mj
13.4
13.1
10.2
9.6
11.2
22.1
26.9
8.8
8.8
8.0
16.6
8.6
8.5
2.7
2.7
3.5
10.8
8.0
6.3
6.2
gr/dscf
0.006
0.006
0.004
0.004
0.005
0.010
0.012
0.004
0.004
0.003
0.007
0.004
0.004
0.001
0.001
0.001
0.005
0.004
0.003
0.003
2-51
-------
TABLE 2-36. COMPARISON OF PARTICULATE CONCENTRATIONS DETERMINED
FROM SAMPLING AT TWO DIFFERENT TEMPERATURES UNDER DCOG UNDERFIRING
CONDITIONS: 316°C (600°F) VS. 121 °C (250°F) BUT ANALYZING
AFTER TREATMENT AT 316°C (600°F)
Test No.
Dl.la
D1.6
D2.5
D2.6
D3.5
D3.6
D4.5
D4.6
D5.5
D5.6
D6.5
D6.6
Date
(1981)
12/8
12/8
12/10
12/10
12/11
12/11
12/12
12/12
12/12
12/12
12/13
12/13
Actual filter
temperature,
°C (°F)
119 (246)
268 (515)
126 (258)
298 (569)
123 (254)
280 (536)
128 (263)
325 (617)
122 (251)
316 (600)
131 (267)
319 (607)
Sequential
heating
temperature,
°C (°F)
316 (600)
-
316 (600)
-
316 (600)
-
316 (600)
-
316 (600)
-
316 (600)
-
Heating
time, h
2
-
2
-
2
-
2
-
2
-
2
-
Front-half catch
particulate
mg
14.6
27.3
15.1
30.3
13.4
25.5
12.3
17.5
2.4
12.9
4.4
9.2
mg/m-*
11.7
28.4
8.2
18.0
7.5
14.8
7.0
10.5
1.4
8.0
2.4
6.3
gr/dscf
0.005
0.012
0.003
0.008
0.003
0.006
0.003
0.004
0.001
0.003
0.001
0.003
aD1.5 was void run sequential heating procedure done on Dl.l.
2-52
-------
2.4 PARTICULATE SULFATE
Acetone rinse residues and filters were analyzed for isopro-
panol (IPA) soluble sulfate (acid sulfate) and water soluble
sulfate (inorganic sulfate). Tables 2-37 and 2-38 summarize the
acid sulfate concentrations determined for the NCOG and DCOG test
series. The IPA extractable acid sulfate concentration is pre-
sented as H-SO. in mg/m . Assuming that the acid sulfate is
hydrated H_SO., the resulting concentration is presented as
H-SO.(H-O)_ in mg/m . Nonsulfate particulate concentration is
determined by subtracting the H-SO.(H-O)2 concentration from the
total particulate concentration.
No water soluble sulfates were found on particulate col-
lected during NCOG underfiring. A few outliers were attributed
to incomplete IPA extraction. Water soluble sulfate data for the
NCOG test series is presented in Appendix C. The water soluble
sulfate found on particulate collected during the DCOG tests are
presented in Table 2-38 as S0,= in mg/m .
2-53
-------
TABLE 2-37. SUMMARY OF PARTICULATE AND ACID SULFATE RESULTS FOR THE NCOG UNDERFIRING TEST SERIES
Test
No.
.1
.2
.3
.4
.5
1.6
2.1
2.2
2.3
2.4
2.5
2.6
3.1
3.2
3.3
3.4
3.5
3.6
4.1
4.2
4.3
4.4
4.5
4.6
5.1
5.2
5.3
5.4
5.5
5.6
6.1
6.2
6.3
6.4
6.5
6.6
Average
filter
temperature.
°C («F)
122 (252)
125 (257)
170 (338)
169 (336)
128 (263)
320 (608)
119 (247)
128 (263)
198 (389)
207 (404)
125 (257)
316 (600)
113 (236)
127 (260)
178 (353)
169 (336)
109 (229)
293 (560)
123 (254)
130 (266)
177 (350)
169 (337)
130 (266)
328 (622)
124 (255)
123 (254)
176 (349)
186 (366)
116 (240)
324 (616)
119 (246)
126 (258)
193 (379)
208 (407)
119 (246)
302 (576)
Conditioning
temperature.
"C (°F)
Ambient
Ambient
177 (350)
Ambient
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
204 (400)
Ambient
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
177 (350)
Ambient
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
204 (400)
Ambient
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
177 (350)
Ambient
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
204 (400)
Ambient
Ambient
Ambient
316 (600)
Ambient
Concentration, nra/m
Rinse
57.7
56.2
19.3
24.7
16.5
57.2
8.7
8.5
49.9
54.1
6.0
22.9
34.0
41.9
6.9
14.1
59.7
37.7
9.0
40.8
12.9
43.3
3.3
10.3
64.9
63.3
14.5
32.2
57.9
27.4
6.4
14.7
50.0
67.6
12.4
20.5
10.8
73.2
6.8
6.6
62.7
65.1
7.0
12.4
9.8
65.5
10.0
12.6
Participate
Filter
71.2
59.2
13.8
18.7
14.3
36.8
12.5
10.5
65.3
45.4
10.5
8.8
8.6
18.7
8.1
9.8
55.7
56.8
11.6
12.8
12.6
56.2
9.5
9.3
76.4
65.3
32.9
33.5
34.9
52.6
39.0
48.1
34.5
56.1
12.1
12.5
11.6
64.1
10.4
9.6
49.5
32.8
8.7
10.2
11.0
53.1
5.6
7.0
Total
128.9
115.4
33.1
43.4
30.8
94.0
21.2
19.0
115.2
99.5
16.5
31.7
42.6
60.6
15.0
23.9
115.4
94.5
20.6
53.6
25.5
99.5
12.8
19.6
141.3
128.6
47.4
65.7
92.2
80.0
45.4
62.8
84.5
123.7
24.5
33.0
22.4
137.3
17.2
16.2
112.2
97.9
15.7
22.6
20.8
118.6
15.6
19.6
Acid su
Rinse
21.7
.
4.4
5.8
1.3
.
0.0
0.0
22.1
.
0.0
8.3
10.0
.
0.0
1.6
23.1
.
0.0
14.8
2.3
.
0.0
2.3
23.2
.
0.4
6.9
11.8
.
0.0
0.0
39.9
.
2.0
6.2
0.0
.
0.0
0.0
29.0
.
0.0
1.8
0.0
.
0.0
0.0
H?SOd
Filter
24.6
-
0.0
0.0
1.6
-
0.0
0.0
16.6
-
0.0
0.0
0.0
-
0.0
0.0
17.1
.
0.0
0.7
0.0
.
0.0
0.0
24.7
.
0.0
0.0
3.0
-
0.0
0.0
12.3
-
0.0
0.0
0.0
.
0.0
0.0
14.3
.
0.0
0.0
0.0
_
0.0
0.0
Total
46.3
-
4.4
5.8
2.9
-
0.0
0.0
38.7
.
0.0
8.3
10.0
-
0.0
1.6
40.2
.
0.0
15.5
2.3
.
0.0
2.3
47.9
.
0.4
6.9
14.8
-
0.0
0.0
52.2
-
2.0
6.2
0.0
-
0.0
0.0
43.3
.
0.0
1.8
0.0
.
0.0
0.0
fate
H?SOa(H70
Rinse
29.7
.
6.1
8.0
1.7
-
0.0
0.0
30.2
-
0.0
11.4
13.7
-
0.0
2.1
31.6
-
0.0
20.2
3.2
.
0.0
3.1
31.8
.
0.6
9.4
16.1
-
0.0
0.0
54.6°
-
2.7
8.5
0.0
.
0.0
0.0
39.7
.
0.0
2.5
0.0
.
0.0
0.0
Filter
33.6
-
0.0
0.0
2.2
.
0.0
0.0
22.8
-
0.0
0.0
0.0
.
0.0
0.0
23.4
.
0.0
1.0
0.0
-
0.0
0.0
33.8
_
0.0
0.0
4.2
-
0.0
0.0
16.7
-
0.0
0.0
0.0
-
0.0
0.0
19.5
.
0.0
0.0
0.0
-
0.0
0.0
?
Total
63.3
-
6.1
8.0
3.9
.
0.0
0.0
53.0
.
0.0
11.4
13.7
.
0.0
2.1
55.0
-
0.0
21.2
3.2
.
0.0
3.1
65.6
.
0.6
9.4
20.3
-
0.0
0.0
71.3
-
2.7
8.5
0.0
-
0.0
0.0
59.2
.
0.0
2.5
0.0
.
0.0
0.0
Honsulfate
paniculate
Rinse
28.0
.
13.2
16.7
14.8
.
8.7
8.5
19.7
.
6.0
11.5
20.3
.
6.9
12.0
28.1
.
9.0
20.6
9.7
.
3.3
7.2
33.1
.
13.9
22.8
41.8
.
6.4
14.7
-4.6
-
9.7
12.0
10.8
-
6.8
6.6
23.0
.
7.0
9.9
9.8
.
10.0
12.6
Filter
37.6
-
13.8
18.7
12.1
.
12.5
10.5
12.3
.
10.5
8.8
8.6
.
8.1
9.8
32.3
.
11.6
11.8
12.6
.
9.5
9.3
42.6
.
32.9
33.5
30.7
.
39.0
48.1
17.8
-
12.1
12.5
11.6
-
10.4
9.6
30.0
.
8.7
10.2
11.0
.
5.6
7.0
Total
65.6
.
27.0
35.4
26.9
.
21.2
19.0
32.0
.
16.5
20.3
28.9
.
1S.O
21.8
60.3
.
20.6
32.4
22.3
.
12.8
16.5
75.7
.
46.8
56.3
72.5
.
45.4
62.8
13.2
-
21.8
24.5
22.4
-
17.2
16.2
53.0
.
15.7
20.1
20.8
.
15.6
19.6
HfSOj
Back-half
5.0
S.6
.
38.9
34.1
.
NAah
426.8b
466a
10.7
_
36.3
13.6
.
M
95.2
4.7
5.2
.
41.2
56.4
NA
.
89.1
11.6
13.5
.
32.0
12.2
-
NA
66.4
21.0
NA
-
53.3
NA
.
NA
83.8
14.6
NA
.
64.2
.
.
.
72.8
Total
51.3
.
44.7
37.0
.
-
.
.
47.7
23.6
.
.
96.8
44.9
.
.
56.7
58.7
.
.
91.4
59.5
-
38.9
27.0
-
-
66.4
73.0
-
-
59.5
-
-
-
83.8
57.9
-
.
66.0
-
-
-
72.8
Ul
*N/A . Not analyzed.
Contaminated with hydrogen peroxide.
cMost likely hydrated with less than two H20 per H?S04 molecule.
-------
TABLE 2-38. SUMMARY OF PARTICULATE AND ACID SULFATE RESULTS FOR THE DCOG UNDERFIRING TEST SERIES
Test
No.
01. 1
01.2
01. 3
01. 4
01.6
02. 1
02.2
02.3
02.4
02.5
02.6
03. 1
03. 2
03.3
03.4
03.5
03.6
04.1
04.2
04.3
04.5
04.6
05.1
05.2
05.3
05.4
05.6
06.1
06.2
06.3
06.4
06.5
06.6
Average
filter
temperature,
°C (°F)
119 (246)
133 (272)
190 (374)
167 (333)
268 (515)
118 (244)
109 (229)
184 (363)
197 (387)
126 (258)
298 (569)
120 (248)
132 (270)
211 (411)
204 (400)
123 (254)
280 (536)
148 (299)
126 (259)
209 (409)
128 (263)
325 (617)
123 (253)
127 (261)
181 (357)
177 (351)
316 (600)
132 (270)
120 (248)
204 (399)
219 (427)
131 (267)
219 (607)
Conditioning
temperature.
•C (°F)
Ambient
316 (600)
Ambient
177 (350)
Ambient
Ambient
Ambient
Ambient
Ambient
177 (350)
Ambient
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
204 (400)
Ambient
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
204 (400)
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
177 (350)
Ambient
Ambient
316 (600)
Ambient
Ambient
Ambient
204 (400)
Ambient
Ambient
Ambient
316 (600)
Ambient
Concentration, ma/m
Participate
Rinse
14.4
3.0
19.8
6.7
14.8
21.1
15.8
73.4b
14.1
7.0
12.3
14.5
13.3
3.4
8.7
18.1
12.0
3.9
13.1
19.0
10.5
2.3
9.7
10.8
21.8
4.8
11.0
11.2
3.4
7.3
10.2
8.5
3.2
7.0
9.4
0.8
4.9
4.6
9.1
1.1
7.4
5.3
6.9
0.5
4.7
Filter
11.7
8.7
13.8
12.9
14.5
17.6
12.6
5.1
7.4
6.8
8.1
6.3
9.0
4.8
9.3
8.0
9.3
7.3
9.0
7.9
9.1
5.2
5.1
6.1
4.9
3.2
5.6
6.6
3.6
3.2
3.2
3.0
1.8
3.4
2.5
0.6
3.1
3.2
4,4
2.4
3.4
2.7
4.0
1.9
1.6
Total
26.1
11.7
33.4
19.6
29.3
38.7
28.4
178.5b
21.5
13.8
20.4
20.8
22.3
8.2
18.0
26.1
21.3
11.2
22.1
26.9
19.6
7.5
14.8
16.9
26.7
8.0
16.6
17.8
7.0
10.5
13.4
11.5
5.0
10.4
11.9
1.4
8.0
7.8
13.5
3.5
10.8
8.0
10.9
2.4
6.3
H7SO*
Rinse
0.0
1.2
0.0
0.0
0.0
1.0
1.0
0.5
0.3
0.0
0.0
0.3
0.1
0.0
1.8
0.0
0.0
0.0
0.0
0.6
0.0
0.0
2.6
0.4
1.9
0.5
0.0
0.2
0.0
0.0
1.0
0.0
0.0
0.2
Fl
0
1
0
0
0
0
1
0
0
0
<0
0.
1
0
0
0
0
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
Su
H?0
ter
0
2
0
0
0
0
0
0
0
0
3
0
4
0
0
0
0
0
0
0
0
0
0
2
0
0
0
0
0
0
0
0
0
0
2
Total
0.0
2.4
0.0
0.0
0.0
1.0
2.0
0.5
0.3
0.0
<0.3
0.3
1.5
0.0
1.8
0.0
0.0
0.0
0.0
0.6
0.0
0.0
2.6
0.6
1.9
0.5
0.0
0.2
0.0
0.0
1.0
0.0
0.0
0.2
fate
sor
Rinse
0.0
1.9
2.1
0.0
1.7
0.6
1.1
2.0
2.7
0.0
:0.0
4.0
0.0
2.9
0.5
0.5
1.3
0.0
0.5
2.1
0.0
0.0
2.1
1.0
1.0
2.4
3.0
0.9
0.0
0.0
0.0
0.0
0.0
0.0
Filter
<0.2
Void
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
<0.2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Total
<0.2
1.9
2.1
0.0
1.7
0.6
1.1
2.0
2.7
0.0
<0.2
4.0
0.0
2.9
0.5
0.5
1.3
0.0
0.5
2.1
0.0
0.0
2.1
1.0
1.0
2.4
0.0
0.9
0.0
0.0
0.0
0.0
0.0
0.0
Total
<0.2
4.3
2.1
0.0
1.7
1.6
3.1
2.5
3.0
0.0
<0.5
4.3
1.5
2.9
2.3
0.5
1.3
0.0
0.5
2.7
0.0
0.0
4.7
1.6
2.9
2.9
0.0
1.1
0.0
0.0
1.0
0.0
0.0
0.2
Nonsulfate
Dartlcula e
Rinse
3.0
3.6
12.7
21.1
15.8
171.8
4.9
9.8
11.5
3.4
8.7
17.8
3.8
13.1
16.7
2.3
9.7
10.8
4.3
8.3
3.4
7.3
5.5
1.8
4.1
6.5
0.8
3.8
4.6
1.1
6.4
5.3
0.5
4.5
Filter
8.5
11.7
14.5
17.6
10.9
5.1
5.8
8.1
6.3
4.8
8.8
4.0
5.9
6.1
7.9
4.7
3.8
6.1
3.2
5.6
3.6
3.2
3.2
1.6
3.4
2.5
0.6
3.1
3.2
2.4
3.4
2.7
1.9
1.6
Total
11.5
15.3
27.2
38.7
26.7
176.9b
10.7
17.9
17.8
8.2
17.5
21.8
9.7
U.2
24.6
7.0
13.5
16.9
7.5
13.9
7.0
10.5
8.7
3.4
7.5
10.0
1.4
7.9
7.8
3.5
9.8
8.0
2.4
6.1
H7SOi
Front-
half
0.0
1.7
0.0
0.0
0.0
0.7
1.5
0.3
0.2
0.0
<0.2
0.2
1.1
0.0
1.3
0.0
0.0
0.0
0.0
0.5
0.0
0.0
1.9
0.5
1.4
0.4
0.0
0.2
0.0
0.0
0.7
0.0
0.0
7.9
TatfT
half
92.0a
3.1
8.0
8.2
6.6
9.8
8.1
&
NAC
6.4
56.8*
4.3
8.6
5.7
NA
7.4
25.0'
9.4
4.5
NAe.
74.7*
5.0
NA
5.0
NA
NA
5.1
8.5
NA
5.2
NA
NA
7.9
Total
92.0*
4.1
8.0
8.2
6.6
10.5
9.«
3os:2*
6.6
57.01
5.4
8.6
7.0
7.4
25.0*
9.4
5.0
;i.7«
6.9
6.4
5.3
8.5
5.9
8.0
Ul
Hydrogen peroxide contaminated.
Contaminated with oil.
CNA « Not analyzed.
-------
2.5 DISCUSSION OF PARTICULATE RESULTS
As shown in Figures 2-1 and 2-2 under similar front-half
temperatures and COG underfiring conditions particulate concen-
trations were consistent between runs. During the NCOG test
series the particulate concentration decreased as the front-half
temperature increased. This decrease was not as marked during
the DCOG test series. Overall, the particulate concentration was
lower during DCOG underfiring than during NCOG underfiring, as
shown in Figure 2-3.
Heat treatment of a particulate catch prior to gravimetric
analysis caused a loss of from 21 to 87 percent, depending on
heating temperature and time, sampling temperature, and type of
COG underfired. As shown in Tables 2-28 through 2-30, more than
half of the total loss caused by a sequential heating takes place
at the first heating.
The results presented in Tables 2-31 through 2-36 are graph-
ically depicted in Figures 2-6 and 2-7. The data shows a con-
sistent difference between samples collected at a specified
temperature and samples collected at a lower temperature and
heated to the specified temperature prior to analysis. The
sequentially heated results are always lower than the actual
filter temperature results.
As shown in Tables 2-37 and 2-38 acid sulfate is a major
constituents of the particulate caught on a 121°C (250°F) heated
2-56
-------
g
I
z
UJ
<_>
z
o
50
40
30
0
§
10
O PART1CULATE FILTER TEMPERATURE
• PARTICULATE FROM SEQUENTIAL HEATING
(RUN 4 EXCLUDED)
177 204
AVERAGE FILTER TEMPERATURE, °C
316
Figure 2-6. Comparison of average participate concentration determined
from sampling at the specified temperature and from sampling at 121°C
(250°F) and analyzing after sequentially heating at specified
temperatures for NCOG underfiring conditions.
2-57
-------
E
E
o:
o
LJ
O
«r
oc
50
40
30
20
10
O PARTICULATE FILTER TEMPERATURE
• PARTICULATE FROM SEQUENTIAL HEATING
177 204
AVERAGE FILTER TEMPERATURE, °C
316
Figure 2-7. Comparison of average participate concentration determined
from sampling at the specified temperature and from sampling at 121°C
(250°F) and analyzing after sequentially heating at specified
temperatures for DCOG underfiring conditions.
2-58
-------
probe and filter collected during NCOG underfiring. Sulfate had
a much smaller impact on particulate caught during DCOG under-
firing. No water soluble sulfate was found on particulate col-
lected during NCOG underfiring. A few outliers were attributed
to incomplete isopropanol extraction.
Average particulate concentration versus average filter
temperature determined from actual sampling temperature, actual
sampling temperature with IPA extraction, and sampling at 171°C
(250°F) with sequential heating prior to analysis are depicted
graphically in Figures 2-8 and 2-9 for NCOG and DCOG underfiring,
respectively. The data indicate actual sampling temperature will
yield a consistently higher concentration than from actual sam-
pling temperature with IPA extraction which will yield a con-
sistently higher concentration than from sequential heating prior
to analysis. The data points averaged at the 177°C (250°F)
filter heat were highly variable whereas the 204°C (400°F) and
316°C (600°F) filter heats yielded more consistent results.
2.5.1 Total Organic Carbon (Filterable) Results
The TOC content of Sampling Train 5 [121°C (250°F) probe/fil-
ter heat] filters was determined by an oxidation/reduction tech-
nique. The TOC content was negligible at all three purge tempera-
tures [177°C (350°F), 232°C (450°F), and 316°C (600°F)] when
compared with the blank filter TOC content. Air and nitrogen
purge blanks for the TOC recovery system averaged 0.9 mg TOC.
Filter blanks averaged 1.5 mg TOC/filter. Sample filters aver-
aged between 1.0 and 2.0 mg TOC/filter. A system recovery
2-59
-------
l_>
z
o
<
o.
UJ
ts
50
40
30
20
10
ONONSULFATE PARTICIPATE AFTER IPA EXTRACTION
APARTICULATE SAMPLED AT 250 THEN HEATED
O PARTICIPATE FROM ACTUAL SAMPLING TEMPERATURE
177 204
AVERAGE FILTER TEMPERATURE, *C
316
Figure 2-8. Comparison of average participate concentration from
actual sampling temperature, sequential heating, and IPA extraction
for NCOG underfiring conditions.
2-60
-------
u
§
a:
a.
LU
o
s
50
40
30
20
10
ONONSULFATE PARTICIPATE AFTER IPA EXTRACTION
A PARTICULATE SAMPLED AT 250 THEN HEATED
DPARTICULATE FROM ACTUAL SAMPLING TEMPERATURE
177 204
AVERAGE FILTER TEMPERATURE, °C
316
Figure 2-9. Comparison of average participate concentration from
actual sampling temperature, sequential heating, and IPA extraction
for DCOG underfiring conditions.
2-61
-------
efficiency of 99 percent was determined by treating a decane-
spiked filter (10 mg by gravimetric analysis) with the oxida-
tion/reduction technique. Actual laboratory data is presented in
Appendix C.
2-6:
-------
2.6 DISCUSSION OF BACK-HALF RESULTS
Sample trains consisted of either a Method 5 back-half for
condensible organics and inorganics determination or a Method 8
back-half for sulfuric acid mist and sulfur dioxide determina-
tion.
2.6.1 Sulfuric Acid Mist
The amount of sulfuric acid measured in the back half of the
sample train during NCOG underfiring is related to the front half
filter/probe temperature. The hotter the filter and probe, the
greater the amount of sulfuric acid mist collected in the back
half. As the results in Tables 2-37 and 2-38 show, the total
sulfuric acid measured by different sampling trains seem to
correlate well. This correlation was not as apparent during DCOG
underfiring where the amount of sulfur in the flue gas was
greatly reduced.
2.6.2 Sulfur Dioxide
The measured SO2 concentration, which stayed relatively
constant throughout each test series, averaged 439 ppm during
NCOG underfiring and 33 ppm during DCOG underfiring. Sulfur
dioxide concentration data were presented in Tables 2-6 through
2-27 for each individual run.
2.6.3 Condensible Organics and Inorganics
The measured condensible organic concentration was constant
throughout both test series. The ampule technique proved to be
much more sensitive than the ether/chloroform extraction. High
biases (attributed to isopropanol contamination) were observed by
the ampule technique but not by the ether/chloroform extraction.
2-63
-------
2.7 REDUCED SULFUR ANALYSIS BY METHOD 15
Table 2-39 presents the results obtained through Method 15
analysis of SRU inlet COG during the NCOG and DCOG underfiring
test series. Hydrogen sulfide (H-S) concentrations averaged 1915
ppm v/v during the NCOG test series, whereas carbonyl sulfide
(COS) averaged <17 ppm, and carbon disulfide (CS2) averaged 34
ppm for an average total reduced sulfur (TRS) concentration of
1961 ppm. Hydrogen sulfide concentrations averaged 5086 ppm
during the DCOG test series, whereas COS averaged <7 ppm and CS2
averaged 80 ppm, for an average TRS concentration of 5112 ppm.
No changes in process operation or conditions (refer to Section
2.10) were recorded between the two test series to corroborate
the large difference in average TRS concentration.
Table 2-40 presents the results obtained through Method 15
analysis of SRU outlet COG during the DCOG underfiring test
series. The SRU was bypassed during NCOG underfiring; therefore,
no outlet data were collected. Hydrogen sulfide concentrations
averaged 7 ppm at the SRU outlet during DCOG underfiring, whereas
COS averaged 19 ppm and CS~ averaged 20 ppm, for an average TRS
of 46 ppm. Sulfur dioxide concentrations at the inlet and outlet
of the SRU averaged <3 ppm during both test series.
Table 2-41 summarizes the results obtained through Method 15
analysis of No. 1 coke battery exit stack gas. Hydrogen sulfide
concentrations averaged <3 ppm during NCOG underfiring; whereas
COS averaged <3 ppm CS_ averaged <2 ppm, for an average TRS of <8
ppm. Hydrogen sulfide, carbonyl sulfide, and carbon disulfide
2-64
-------
TABLE 2-39. SUMMARY OF RESULTS OBTAINED THROUGH METHOD 15
ANALYSIS OF SRU INLET COG
Bag sample
collection
Date
(1981)
Time
Corresponding
participate
Run No.
Analysis
Date
(1981)
Time
Concentration, ppm
H2S
COS
CS2a
SO 2
TRS
NCOG TEST SERIES
10/27
10/27
10/28
10/28
10/29
10/29
10/30
10/30
0930
1430
0930
1605
0930
1400
1000
1500
1
2
3
4
5
6
7
8
10/27
10/28
10/27
10/28
10/30
10/28
10/28
10/28
10/29
10/29
10/30
10/30
1000
1354
1535
1442
1550
1036
1420
1642
1118
1454
1042
1606
Average
2000
2100
3800
1440
1800
1770
2200
1700
1500
1320
1590
1770
1915
130
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<17
44
48
31
34
39
40
40
39
32
<2
31
33
34
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
3
2174
2148
3831
1474
1839
1810
2240
1739
1532
1320
1621
1803
1961
DCOG TEST SERIES
12/8
12/9
12/10
12/10
12/11
12/11
12/11
1230
1150
1130
1455
0740
1215
1005
Dl
-
-
D2
-
D3
D4
12/8
12/10
12/10
12/10
12/11
12/11
12/12
1718
1318
1336
1712
1600
1624
1224
Average
2300
6600
8700
5700
4300
5600
2400
5086
<5
21
<5
<5
<5
<5
<5
<7
62
54
58
190
72
68
60
80
<6
<6
<6
<6
<6
<6
<6
<6
2362
6675
8758
5890
4372
5268
2460
5112
reported as S02 (twice C$2 value detected).
2-65
-------
TABLE 2-40. SUMMARY OF RESULTS OBTAINED THROUGH METHOD 15
ANALYSIS OF SRU OUTLET COG DURING DCOG UNDERFIRING
Bag sample
collection
Date
(1981)
12/8
12/9
12/10
12/10
12/11
12/11
12/12
12/12
Time
1230
1150
1130
1455
0740
1215
0755
1005
Corresponding
participate
Run No.
Dl
-
-
D2
-
D3
-
D4
Analysis
Date
(1981)
12/8
12/9
12/10
12/10
12/10
12/11
12/11
12/12
12/11
12/11
12/12
Time
1412
1400.
1248°
1212
1624
1318
1436
1142
1412
1018
1054
Average
Concentration, ppm
H2S
112
6
<2
4
6
9
9
6
14
2
4
7
COS
25
21
18
20
20
18
18
20
19
19
19
19
cs2a
24
20
14
18
20
22
22
17
20
21
20
20
SO 2
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
TRS
61
47
32
42
46
46
49
43
53
42
43
46
JCS2 reported as S02 (twice CS2 value detected)
DNot used in average.
2-66
-------
TABLE 2-41. SUMMARY OF RESULTS OBTAINED THROUGH METHOD 15
ANALYSIS OF NO. 1 COKE BATTERY EXIT STACK GAS
Bag sample
collection
Date
(1981)
Time
Corresponding
participate
Run No.
Analysis
Date
(1981)
Time
Concentration, ppm
H2S
COS
re a
CS2
SO 2
TRS
NCOG TEST SERIES
10/27
10/27
10/28
10/28
10/29
10/29
10/30
10/30
0930
1430
0930
1605
0930
1400
1000
1500
1
2
3
4
5
6
7
8
10/27
10/27
10/30
10/28
10/28
10/29
10/29
10/30
10/30
1200
1606
1436
1112
1706
1218
1600
1124
1736
Average
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
<3
4
5
<2
<2
<2
<2
<2
<2
<2
<2
180
280
64
280
360
260
190
300
210
236
4
5
<8
<8
<8
<8
<8
<8
<8
<8
DCOG TEST SERIES
12/8
12/10
12/11
12/12
1230
1330
1400
1030
Dl
D2
D3
D4
12/8
12/10
12/11
12/11
12/12
1500
1430
1536
1500
1106
Average
<2
<2
<2
<2
<2
<2
<2
<2
<2
<2
<2
<2
<2
<2
<3
<2
<2
<2
7
18
3
<3
<3
9
<6
<6
<6
<6
<6
<6
CS2 reported as S02 (twice CS2 value detected).
2-67
-------
concentrations all averaged <2 ppm during DCOG underfiring, for
an average TRS concentration of <6 ppm.
According to Method 15 analysis, sulfur dioxide concentra-
tions averaged 236 ppm during NCOG underfiring and 9 ppm during
DCOG underfiring; however, Method 8 analysis showed an average
sulfur dioxide concentration of 439 ppm during NCOG underfiring
and 33 ppm during DCOG underfiring.
Harmon Engineering and Testing provided analytical services
for determination of reduced-sulfur constituents of selected flue
gas samples by EPA Method 15.* The major modification made to
Method 15 was the analysis of gas bag samples instead of the
usual gas samples continuously extracted via heat-traced Teflon
tubing. The highly explosive nature of COG and the great distance
between the three sample sites necessitated this modification.
Method 15 uses gas chromatographic separation and flame photo-
metric detection to determine the reduced-sulfur constituents and
sulfur dioxide concentrations.
The FPD used has a linear response range up to 70 ppm.
Self-absorption of the sulfur molecular light occurs at higher
concentrations and reduces the slope of the line. Figure 2-10
presents a typical H.S calibration curve as the concentration
increases. Having a dynamic dilution system prior to the sample
loop is the preferred method for staying in the FPD linear range.
Because the COG bag sample could not be diluted prior to analy-
sis, the sample loop size was reduced. Reduction in sample size
*40 CFR 60, Appendix A, Reference Method 15, July 1980.
2-68
-------
20,000
10,000 -
7,000 -
5,000 -
3,000 -
2,000 -
o
1^
x 1,000
»/l
=i 700
-------
also lowers FPD sensitivity and accuracy. Analysis of the COG
inlet sample required a factor of 22 reduction in sample loop
size over calibration loop size. Because response was still
above the FPD linear response range, self-absorption of the
sulfur molecular light is the most likely reason for the high TRS
values resulting from the use of Method 15 at the SRU inlet. As
self-absorption occurs and the slope of the response versus
concentration curve decreases, a relatively small increase in
response is interpreted as a large increase in concentration.
True calibration in this region of the curve is not possible.
The data show an increase in the COS concentration through the
SRU during DCOG underfiring. This is most probably due to the
small sample loop used for inlet analysis, which was 22 times
smaller than the outlet (calibration) loop.
2-70
-------
2.8 GAS STREAM FLOW RATE AND COMPOSITION
Tables 2-42 and 2-43 summarize the flue gas conditions data
collected at the No. 1 coke battery exit stack during the NCOG
and DCOG underfiring test series. Actual volumetric flow rates
are expressed in cubic meters per hour (m /h) and actual cubic
feet per hour (acfh) at stack conditions. Flow rates corrected
to standard conditions [20°C and 760 mmHg (68°F and 29.92 in.Hg)
and zero percent moisture] are expressed as dry normal cubic
meters per hour (dNm /h) and dry standard cubic feet per hour
(dscfh).
Prior to the first test run of each series a full velocity
traverse was performed. Table 2-44 details the data collected
from these full velocity traverses. Before the NCOG test series,
the volumetric flow rate averaged 45,845 dNm /h (1,619,014
dscfh), and the stack temperature averaged 240°C (464°F). Prior
to the DCOG test series, the volumetric flow rate was measured at
44,134 dNm /h (1,558,567 dscfh), and the stack temperature was
228°C (443°F).
The particulate sampling train nozzles were placed in the
stack at an accessible point of average velocity, as determined
by the preliminary velocity traverse. This position was main-
tained throughout the test period. Velocity head and stack
temperature were recorded every 10 minutes. Sample trains were
operated simultaneously, with few exceptions, within each run.
Tables 2-42 and 2-43 also contain all sample train start and stop
times.
2-71
-------
TABLE 2-42. SUMMARY OF FLUE GAS CONDITIONS DURING NCOG UNDERFIRING TESTING
Run No.
1-1
1-2
1-3
1-4
1-5
1-6
Date
(1981)
10/27
Sampling
period
0910-1110
0914-1114
0910-1110
0914-1114
0947-1057
0958-1102
Average (Q)
(6)
2-1
2-2
2-3
2-4
2-5
2-6
10/27
1355-1555
1358-1558
1355-1555
1358-1558
1424-1624
1419-1549
Average (Q)
(6)
3-1
3-2
3-3
3-4
3-5
3-6
10/28
0955-1155
0958-1158
0955-1155
0958-1158
0947-1147
0950-1150
Average (Q)
(6)
Flue gas flow rate
, Actual3
mj/h
106,960
106,651
107,648
106,381
94,721
92,677
106,910
102,506
94,325
94,566
94,240
94,471
98,622
98,086
94,400
95,718
102,955
102,650
103,600
102,839
113,803
115,055
103,011
106,817
acfh
3,777,241
3,766,316
3,801,518
3,756,791
3,345,007
3,272,822
3,775,466
3,619,949
3,331,033
3,339,559
3,328,042
3,336,176
3,482,787
3,463,857
3,333,702
3,380,242
3,635,799
3,625,039
3,658,571
3,631,694
4,018,903
4,063,123
3,637,776
3,772,188
, Standard
dNmJ/h
48,666
48,106
47,148
48,616
42,057
46,661
48,134
46,876
42,173
42,266
42,288
42,449
46,059
47,253
42,294
43,748
47,583
47,844
46,258
47,406
53,499
50,694
47,273
48,881
dscfh
1,718,626
1,698,840
1,665,014
1,716,865
1,485,228
1,647,806
,699,836
,655,397
,489,327
,492,594
,493,373
,499,060
,626,567
,668,717
,493,589
,544,940
,680,373
,689,592
,633,571
,674,132
,889,290
,790,217
,669,417
,726,196
Moisture,
V
ft
12.3
12.9
15.6
11.8
13.5
1.7C
13.2
13.2
13.7
13.1
13.5
12.6
13.5
10.8
13.2
12.9
12.2
11.0
15.1
12.0
12.3
17.8
12.6
13.4
Temperature
°C
280
281
280
281
288
288
281
283
279
284
279
283
259
259
281
274
279
282
280
282
270
270
281
277
°F
537
538
536
538
550
550
537
542
535
543
534
542
499
499
539
525
535
540
536
540
518
518
538
531
Carbon
dioxide, %
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
.2
.2
.2
.2
.2
4.2
4.2
2.3
2.3
2.3
2.3
2.3
2.3
2.3
2.3
Oxygen,
V
-------
TABLE 2-42 (continued)
Run No.
4-1
4-2
4-3
4-4
4-5
4-6
Date
(1981)
10/28
Sampling
period
1540-1716
1543-1718
1540-1715
1543-1715
1423-1706
1427-1716
Average (Q)
(6)
5-1
5-2
5-3
5-4
5-5
5-6
10/29
0940-1137
0943-1133
0940-1135
0943-1135
0943-1137
0942-1137
Average (Q)
(6)
6-1
6-2
6-3
6-4
6-5
6-6
10/29
1350-1550
1353-1553
1350-1550
1354-1554
1353-1553
1352-1552
Average (Q)
(6)
Flue gas flow rate
, Actual3
nT/h
99,070
99,108
98,964
100,893
113,770
113,495
99,509
104,217
99,656
104,659
100,065
99,119
109,724
109,572
100,875
103,799
94,435
94.734
94,514
95,053
109,673
109,786
94,684
99,699
acfh
3,498,604
3,499,941
3,494,845
3,562,981
4,017,725
4,008,004
3,514,093
3,680,350
3,519,316
3,695,966
3,533,728
3,500,352
3,874,861
3,869,468
3,562,340
3,665,615
3,334,937
3,345,471
3,337,721
3,356,748
3,873,037
3,877,050
3,343,719
3,520,827
, Standard
dNmJ/h
45,089
45,340
45,107
44,301
52,065
52,670
44,959
47,429
46,117
48,088
45,624
45,544
50,546
50,881
46,358
47,800
43,298
43,042
43,511
42,503
50,314
50,346
43,089
45,502
dscfh
,592,304
,601,155
,592,934
,564,464
,838,631
,860,026
,587,714
,674,919
,628,613
,698,186
,611,199
,608,375
,785,009
,796,847
,636,593
,688,038
1,529,041
1,520,006
1,536,556
1,500,961
1,776,813
1,777,953
1,521,641
1,606,888
Moisture,
14.4
13.6
14.4
14.3
14.7
13.5
14.2
14.2
13.3
13.5
14.2
13.7
14.1
13.4
13.7
13.7
14.0
14.4
13.3
15.6
14.7
14.5
14.3
14.4
Temperature
°C
275
277
274
276
270
270
276
274
274
276
276
275
271
271
275
274
274
277
277
278
271
271
277
275
°F
527
531
525
529
518
518
528
525
524
529
529
527
520
520
527
525
526
530
530
532
520
520
530
526
Carbon
dioxide, %
4.
4.
4.
4.
4.
4.
4.
4.
4.3
4.3
4.3
4.3
4.3
4.3
.3
.3
.5
.5
.5
.5
.5
.5
4.5
4.5
Oxygen,
%
11.0
11.0
11.0
11.0
11.0
11.0
11.0
11.0
11.3
11.3
11.3
11.3
11.3
11.3
11.3
11.3
10.5
10.5
10.5
10.5
10.5
10.5
10.5
10.5
-J
UJ
(continued)
-------
TABLE 2-42 (continued)
Run No.
7-1
7-2
7-3
7-4
7-5
7-6
Date
(1981)
10/30
Sampling
period
0930-1130
0933-1133
0930-1130
0933-1133
0935-1135
0934-1134
Average (Q)
(6)
8-1
8-2
8-3
8-4
8-5
8-6
10/30
1438-1638
1441-1641
1438-1638
1441-1641
1439-1623
1438-1608
Average (Q)
(6)
Flue gas flow rate
, Actual3
mj/h
100,034
100,343
103,699
100,267
109,520
109,489
101,086
103,892
101,278
101,279
100,996
101,273
109,733
109,966
101,206
104,088
acfh
3,532,635
3,543,545
3,662,069
3,540,882
3,867,652
3,866,549
3,569,783
3,668,889
3,576,587
3,576,610
3,566,612
3,576,390
3,875,168
3.883,405
3,574,050
3,675,795
, Standard
dNmJ/h
46,329
46,251
44,544
46,386
51,078
51,147
45,878
47,623
45,435
45,173
46,068
45,672
50,667
50,152
45,587
47,195
dscfh
,636,079
,633,313
,573,041
,638,107
,803,803
,806,240
,620,135
,515,097
,604,520
,595,254
,626,862
,612,867
,789,295
,771,103
,609,876
,666,650
Moisture,
%
12.9
12.8
13.4
12.5
13.2
13.0
12.9
13.0
14.4
15.2
12.9
13.7
14.1
15.1
14.1
14.2
Temperature
°C
277
280
277
280
271
271
279
276
285
283
285
286
271
271
285
280
°F
530
537
530
536
520
520
533
529
545
542
545
547
520
520
545
537
Carbon
dioxide, %
4.0
.0
.0
.0
.0
.0
.0
.0
4.3
4.3
4.3
4.3
4.3
4.3
4.3
4.3
Oxygen,
%
11.0
11.0
11.0
11.0
11.0
11.0
11.0
11.0
9.3
9.3
9.3
9.3
9.3
9.3
9.3
9.3
to
•o
aVolumetric flow rate in actual cubic meters per hour (m /h) and actual cubic feet per hour (acfh) at stack conditions.
Volumetric flow rate in dry normal cubic meters per hour (dNm/h) and dry standard cubic feet per hour (dscfh): Standard
conditions = 20°C and 760 mm Hg (68°F and'29.92 in. Hg) and zero percent moisture.
C0utlier - not used in calculations.
Average (Q) Is average quad train tests.
Average (6) is average of all six tests.
-------
TABLE 2-43. SUMMARY OF FLUE GAS CONDITIONS DURING DCOG UNDERFIRING TESTING
Run No.
01-1
01 -2
01-3
01 -4_
01 -5C
01-6
Date
(1981)
12/8
Sampling
period
1205-1335
1208-1338
1205-1335
1208-1338
1209-1339
Average (Q)
(5)
02-1
02-2
D2-3
02-4
D2-5
02-6
12/10
1341-1511
1308-1508
1310-1510
1312-1512
1310-1510
1311-1511
Average (Q)
(6)
03-1
03-2
03-3
03-4
D3-5
D3-6
12/11
1131-1540
1134-1540
1134-1542
1139-1548
1145-1544
1137-1546
Average (Q)
(6)
Flue gas flow rate
, Actual3
mj/h
90,548
90,863
91,316
91,309
80,795
91,009
88,966
102,820
103,171
103,773
103,721
98,778
98,700
103,371
101,827
84,440
84,484
86,574
86,156
94,944
95,278
85,414
88,646
acfh
3,197,639
3,208,783
3,224,786
3,224,520
2,853,244
3,213,932
3,141,794
3,631,049
3,643,425
3,664,702
3,662,869
3,488,292
3,485,548
3,650,511
3,595,981
2,981,939
2,983,501
3,057,331
3,042,559
3,352,885
3,364,702
3,016,332
3,130,486
n Standard
dNmJ/h
45,170
44,444
44,715
44,920
39,471
44,812
43,744
49,481
49,815
49,927
50,043
47,600
47,775
49,817
49,107
41,798
41,491
41,852
42,185
47,202
46,443
41,832
43,495
dscfh
1,595,142
1,569,507
1,579,103
1,586,320
1,393,914
,582,518
,544,797
,747,391
,759,182
,763,133
,767,255
,680,969
,687,140
,759,240
,734,178
,476,086
,465,237
,477,970
,489,756
,666,931
,640,093
,477,262
,536,012
Moisture,
%
9.9
11.7
11.6
11.0
10.2
11.1
10.9
12.2
12.0
12.3
12.1
12.2
11.8
12.2
12.1
9.9
10.6
12.0
11.5
9.5
11.3
11.0
10.8
Temperature
°C
242
242
242
243
252
242
244
253
252
252
252
252
252
252
252
252
252
252
249
252
252
251
252
°F
468
468
468
470
485
469
472
487
486
486
486
486
486
486
486
486
486
486
480
486
486
486
486
Carbon
dioxide, %
4.5
4.5
4.5
4.5
4.5
.5
.5
.3
.3
.3
.3
4.3
4.3
4.3
4.3
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
Oxygen,
%
9.4
9.4
9.4
9.4
9.4
9.4
9.4
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.0
12.0
12.0
12.0
12.0
12.0
12.0
12.0
1/1
(continued)
-------
TABLE 2-43 (continued)
Run No.
D4-1
D4-2
04-3.
D4-4C
D4-5
D4-6
Date
(1981)
12/12
Sampling
period
0940-1140
0943-1143
0940-1140
0940-1140
0942-1142
Average (Q)
(5)
D5-1
D5-2
05-3
05-4
05-5
05-6
12/12
1404-1604
1407-1607
1358-1558
1400-1600
1358-1558
1359-1559
Average (Q)
(6)
06-1
06-2
06-3
06-4
06-5
06-6
12/13
0945-1145
0947-1147
0945-1145
0947-1147
0945-1145
0946-1146
Average (Q)
(6)
Flue gas flow rate
, Actual3
mj/h
91,867
91,898
92,085
94,584
94,488
91,950
92,984
93,540
93,658
94,219
94,313
90,983
90,680
93,932
92,899
86,817
87,102
86,868
86,712
88,151
88,127
86,875
87,296
acfh
3,244.223
3,245,338
3,251,926
3,340,189
3,336,804
3,247,162
3,283,696
3,303,306
3,307,488
3,327,285
3,330,605
3,213,030
3,202,302
3,317,171
3,280,669
3,065,894
3,075,958
3,067,686
3,062,194
3,112,999
3,112,161
3,067,933
3,082,815
, Standard
dNmJ/h
44,981
44,895
44,617
45,882
46,101
44,831
45,295
46,412
46,137
46,292
46,074
44,907
45,615
46,229
45,906
43,962
43,438
43,837
43,681
44,327
44,383
43,730
43,938
dscfh
1,588,494
1,585,451
1,575,619
1,620,295
1,628,021
1,583,188
1,599,576
1,639,024
1,629,300
1,634,772
1,627,070
1,585,882
1,610,872
1,632,542
1,621,153
1,552,508
1,534,002
1,548,066
1,542,579
1,565,391
1,567,349
1,544,289
1,551,649
Moisture,
%
11.0
11.2
11.8
11.9
11.4
11.3
11.5
11.8
12.5
12.7
13.2
12.3
10.6
12.6
12.2
11.6
12.8
11.9
12.6
12.2
12.1
12.2
12.2
Temperature
°C
254
254
256
254
254
255
254
244
244
244
244
244
244
244
244
235
236
235
232
235
235
235
235
°F
490
490
492
490
490
491
490
471
471
471
471
471
471
471
471
455
457
455
449
455
455
454
454
Carbon
dioxide, %
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
3.7
5.1
5.
5.
5.
5.
5.
5.
5.
Oxygen,
%
11.
11.
11.
11.
11.
11.
11.
11.8
11.8
11.8
11.8
11.8
11.8
11.8
11.8
11.0
11.0
11.0
11.0
11.0
11.0
11.0
11.0
aVolumetr1c flow rate In actual cubic meters per hour (m /h) and actual cubic feet per hour (acfh) at stack conditions.
''Volumetric flow rate In dry normal cubic meters per hour (dfhn3/h) and dry standard cubic feet oer hour (dscfhl:
Standard conditions = 20°C and 760 mm Hg (68°F and 29.92 in. Hg) and zero percent moisture.
cTest voided due to excessive post-test leak rate.
Average (Q) is average quad train tests.
Average (5) or (6) is average of all five or six tests.
-------
TABLE 2-44. SUMMARY OF FLUE GAS FLOW RATE AND TEMPERATURE
AS MEASURED BY A FULL VELOCITY TRAVERSE
Run No.
Date
(1981)
Flue gas flow rate
Actual3
m3/h acfh
Standard13
dNm^/h
dscfh
Temperature
°C
°F
NCOG underfiring test series
Pre. 1
Pre. 2
V.T.
10/22
10/22
10/27
Average
93,236
89,465
95,169
92,623
3,292,608
3,159,420
3,360,858
3,270,962
47,368
44,999
45,169
45,845
1,672,794
1,589,130
1,595,118
1,619,014
228
233
259
240
442
451
499
464
DCOG underfiring test series
Pre.
12/7
86,169
3,043,045
44,134
1,558,567
228
443
aVolumetric flow rate in actual cubic meters per hour (m /h) and actual cubic
feet per hour (acfh) at stack conditions.
Volumetric flow rate in dry normal cubic meters per hour (dNm /h) and dry
standard cubic feet per hour (dscfh): Standard conditions = 20°C and 760
mmHg (68°F and 29.92 in.Hg) and zero percent moisture.
2-77
-------
During the NCOG underfiring test series, the volumetric flow
rate averaged 46,882 dNm /h (1,634,766 dscfh), temperature aver-
aged 277°C (531°F), and moisture content averaged 13.6 percent.
Oxygen and carbon dioxide contents averaged 10.6 and 4.0 percent,
respectively.
During the DCOG underfiring test series, the volumetric flow
rate averaged 45,247 dNm /h (1,597,894 dscfh), temperature aver-
aged 247°C (476°F), and the moisture content averaged 11.6 per-
cent. Oxygen and carbon dioxide contents averaged 11.3 and 4.2
percent, respectively.
2-78
-------
2.9 VISIBLE EMISSIONS
Table 2-45 summarizes visible emissions data collected
during the NCOG underfiring test series. Data were not collected
during Runs 1, 2, and 3. During Run 4, opacities ranged from 0
to 45 percent and averaged 15 percent. These opacities were
markedly higher than those during Runs 5 through 8, which ranged
from 0 to 40 percent and averaged 3 percent. Frank Clay of the
EPA made the visible emissions observations.
Extreme adverse weather conditions prevented the observation
of visible emissions during the DCOG underfiring test series.
Cloud cover was 100 percent during the entire test series, and
snow fell during most of the test series.
2-79
-------
TABLE 2-45. SUMMARY OF VISIBLE EMISSIONS DATA NUMBER 1 COKE BATTERY EXIT STACK, NCOG UNDERFIRING TEST SERIES
Particulate
Run No. .
1
2
3
4
5
6
Date
(1981)
10/27
10/27
10/28
10/28
10/29
10/29
Particulate
test time
0910-1114
1355-1624
0955-1158
1423-1716
0940-1137
1350-1554
Corresponding
VE run No.
N/Aa
N/A
N/A
VE-1
VE-2
VE-4
VE set
No.
VE-1-1
VE-1-2
VE-1 -3
VE-1 -4
VE-1-5
VE-1 -6
VE-1 -7
VE-1 -8
VE-1 -9
VE-1-10
VE-2-1
VE-2-2
VE-2-3
VE-2-4
VE-2-5
VE-2-6
VE-2-7
VE-2-8
VE-2-9
VE-2-10
VE-4-1
VE-4-2
VE-4-3
VE-4-4
VE-4-5
VE-4-6
VE-4-7
VE observation
time
1455-1500
1501-1506
1507-1512
1513-1518
1519-1525
1526-1531
1532-1537
1538-1543
1544_1549
1550-1551°
1035-1040
1041-1046
1047-1052
1053-1058
1059-1104
1105-1110
1111-1116
1117-1122
1123-1128
1129-1134
1431-1436
1437-1442
1443-1448
1449-1454
1455-1500
1501-1506
1507-1512
Average
% opacity
30
11
7
10
17
10
16
17
18
10
6
3
3
2
2
0
0
0
0
0
1
0
0
0
2
0
0
Range
20-45
0-35
0-15
0-25
10-25
5-20
0-25
10-20
10-20
5-15
5-10
0-5
0-5
0-5
0-5
0
0
0
0
0-5
0-5
0
0
0-5
0-5
0
0
00
o
(continued)
-------
TABLE 2-45 (continued)
Participate
Run No.
6
(cont'd)
7
8
Date
(1981)
10/29
10/30
10/30
Particulate
test time
1350-1554
0930-1135
1438-1641
Corresponding
VE run No.
VE-4
VE-5
VE-6
VE-7
VE set
No.
VE-4-8
VE-4-9
VE-4-10
VE-5-1
VE-5-2
VE-5-3
VE-5-4
VE-5-5
VE-5-6
VE-5-7
VE-5-8
VE-6-1
VE-6-2
VE-6-3
VE-6-4
VE-6-5
VE-6-6
VE-7-1
VE-7-2
VE-7-3
VE-7-4
VE-7-5
VE-7-6
VE-7-7
VE-7-8
VE-7-9
VE-7-10
VE observation
time
1513-1518
1519-1524
1525-1530
1536-1541
1542-1547
1548-1553
1554-1559
1600-1605
1606-1611
1612-1617.
1618-1620^
1003-1008,
1011-1012°
1018-1023
1024-1029
1030-1035.
1036-1040
1443-1448
1449_1454
1455-1500
1501-1506
1507-1512
1513-1518
1519-1524
1525-1530
1531-1536f
1540-1544
Average
% opacity
0
0
3
8
<6
<18
9
<2
0
0
0
0
0
0
<5
<2
0
<6
<3
<2
<6
8
<6
<5
<5
<7
<5
Range
0
0-5
0-10
5-10
<5-20
0-40
0-20
0-5
0
0
0
0
0
0-5
<5-5
0-<5
0
0-15
0-5
0-5
0-15
5-10
0-10
0-10
<5-10
0-15
0-10
I
00
(continued)
-------
TABLE 2-45 (continued)
Particulate
Run. No.
8
(cont'd)
Date
(1981)
10/30
Particulate
test time
1438-1641
Corresponding
VE run No.
VE-8
VE set
No.
VE-8-1
VE-8-2
VE-8- 3
VE-8-4
VE-8- 5
VE-8-6
VE-8-7
VE-8-8
VE-8-9
VE-8-10
VE observation
time
1551-1556
1557-1602
1603-1608
1609-1614
1615-1620
1621-1626
1627-1632
1633-1638
1639-1644
1645-1650
Average
% opacity
11
<3
0
0
0
0
2
8
<5
<5
Range
<5-20
0-5
0
0
0
0
0-15
5-10
0-10
0-5
Ni
I
00
to
aN/A = Not analyzed.
Two-minute set.
cThree-minute set.
Two-minute set.
eThree-minute set.
Five-minute set.
-------
2.10 PROCESS DATA
During each test, the process operation was monitored by an
MRI representative. Tables 2-46 and 2-47 summarize the process
data collected during the NCOG and DCOG test series, respec-
tively. The following parameters were monitored: average COG to
battery average coal in battery, number of pushes and charges,
number of ovens empty, and exhaust main pressure (push and coke
side).
Average COG to Battery No. 1 during the NCOG underfiring
testing was 4,820 m3/h (170,190 ft3/h). The coal in the battery
averaged 640.4 Mg (706.1 tons). There were an average of 6
pushes, 7 charges, and 4 empty ovens during a test run. Exhaust
main pressure averaged 78 mmH-O (3.1 in.H-O) on the push side,
and 81 mmH-O (3.2 in.H^O) on the coke side.
Average COG to Battery No. 1 during the DCOG underfiring
testing was 4,339 m3/h (153,210 ft3/h). The coal in the battery
averaged 596.4 Mg (567.7 tons). There were an average of 6
pushes, 5 charges, and 3 empty ovens during a test run. Exhaust
main pressure averaged 57 mmH-O (2.2 in.H2O) on the push side,
and 60 mmH-O (2.4 in.H20) on the coke side.
Tables 2-48 and 2-49 summarize the sulfur content of the
coal and coke during the NCOG and DCOG test series. During the
NCOG test series, the coal and the coke contained an average of
0.82 and 0.70 percent sulfur, respectively. During the DCOG test
series, the coal averaged 0.80 percent sulfur, and the coke
averaged 0.72 percent sulfur.
2-83
-------
TABLE 2-46. NCOG TEST SERIES PROCESS DATA0
to
I
00
Run No.
1
2
3
4
5
6
7
8
Date
(1981)
10/27
10/27
10/28
10/28
10/29
10/29
10/30
10/30
Time
0910-1114
1355-1624
0947-1158
1423-1718
0940-1137
1350-1554
0930-1135
1438-1641
Average
Average COG
to battery"
m3/h
4874
4754
4117
5012
4990
5213
4528
5068
4820
ftj/h
1/2,120
167,880
145,390
176,990
176,220
184,070
159,880
178,940
170,190
Average coal
in battery
Mg
604.6
622.7
635.1
655.2
650.3
650.4
648.1
657.2
640.4
tons
666.6
686.6
700.2
722.4
717.0
717.1
714.6
724.6
706.1
No. of
pushes
12
4
6
9
7
5
3
4
6
No. of
charges
12
3
5
11
6
7
6
4
7
No. of
ovens empty
6
6
3
3
3
3
3
3
4
Exhaust main pressure
Push side
mmH^O
78
74
76
78
79
79
80
79
78
in.H20
3.1
2.9
3.0
3.1
3.1
3.1
3.1
3.1
3.1
Coke side
nmH20
80
82
83
81
81
80
80
80
81
in.HzO
3.1
3.2
3.2
3.2
3.2
3.1
3.1
3.1
3.2
aThe following information was provided by Republic Steel Corporation: 1) Average amount of coal charged per coke
oven: -15.3 tons/coking cycle. 2) Average amount of coke produced per coke oven: -10.2 tons/coking cycle.
3) Coking temperature: -2300°F. (This is the temperature recorded in the flues. The temperature of the coke would
be approximately 150°F lower.) 4) Average coking time: -20.5 hours.
bAt 40°C (140°F).
-------
TABLE 2-47. DCOG TEST SERIES PROCESS DATAC
Run No.
D-1
D-2
D-3
0-4
D-5
0-6
Date
(1981)
12/8
12/10
12/11
12/12
12/12
12/13
Time
1150-1352
1305-1512
1134-1142
1350-1548
0940-1145
1355-1607
0945-1147
Average
Average COG
to batteryb
m^/h
4591
4521
4234
4130
4348
4209
4339
ftj/h
162,100
159,640
149,520
145,850
153,530
148,620
153,210
Average coal
in battery
Mg
598.6
598.6
585.9
598.6
598.6
598.6
596.4
tons
660.0
660.0
646.0
660.0
660.0
660.0
657.7
No. of
pushes
11
7
4
4
3
5
6
No. of
charges
10
8
4
3
2
5
5
No. of
ovens empty
3
3
3
3
3
3
3
Exhaust main pressure
Push side
rnrnHpO
64
62
55
55
55
52
57
in.HpO
2.5
2.4
2.2
2.2
2.2
2.0
2.2
Coke side
nfnH20
62
65
55
60
60
60
60
in.H20
2.4
2.6
2.2
2.2
2.4
2.4
2.4
00
Ul
The following information was provided by Republic Steel Corporation: 1) Average amount of coal charged per coke oven:
-14 tons/coking cycle during November/December. 2) Average amount of coke produced per coke oven: -10 tons/cokinq
cycle during November/December. 3) Coke temperature: ~2175°F to 2250°F. (This is the temperature recorded in the
flues. The temperature of the coke would be approximately 150°F lower.) 4) Average coking time: -24 hours. 5) Btu
content of DCOG: 540 Btu/scf.
bAt 40°C (104°F).
-------
TABLE 2-48. SULFUR CONTENT OF COAL AND COKE DURING
NCOG TESTS (PERCENT)
Date analyzed3
10/25/81
10/26/81
10/27/81
10/28/81
10/29/81
10/30/81
Average
Coal
0.75
0.77
0.98
0.80
0.78
0.85
0.82
Coke
0.70
0.72
0.75
0.65
0.70
0.65
0.70
TABLE 2-49. SULFUR CONTENT OF COAL AND COKE DURING
DCOG TESTS (PERCENT)
Date analyzed3
12/07/81
12/08/81
12/09/81
12/10/81
12/11/81
12/12/81
12/13/81
Average
Coal
0.78
0.78
0.83
0.80
0.78
0.87
0.80
0.80
Coke
0.78
0.75
0.73
0.68
0.68
0.70
0.70
0.72
Sulfur content of coal is usually analyzed 1 to 2 days before the
coal is charged to the ovens. Sulfur content of coke is usually
analyzed the same day the coke is pushed from the ovens.
2-86
-------
The MRI process description and data as received by PEDCo
are included in Appendix I.
2-87
-------
SECTION 3
PROCESS DESCRIPTION
The Republic Steel facility in Cleveland currently operates
three Koppers gun-flue coke oven batteries. The testing was
conducted on the flue gas from the No. 1 coke oven battery, which
consists of 51 ovens. Coke was first pushed from this battery in
January 1977. Initial startup of the Sulfiban desulfurization
system was in March/April 1981. Coke is produced continuously
24-hours per day. This facility uses byproduct coke ovens to
produce furnace coke from coal; the coke is used in blast furnaces
for the reduction of iron ore to metallic iron. Figure 3-1 is a
simplified process flow diagram.
The gas collecting system has two offtakes, one located at
each end of the oven. The volatile products liberated during the
coking process pass through the battery's dual collection main
and are processed by the byproduct recovery system, which con-
sists of a primary cooler, exhauster, detarrer, ammonia absorber,
final cooler, a benzol scrubber, Sulfiban desulfurization system,
pressure regulator, and booster. After leaving the byproduct
recovery system, the normal or desulfurized coke oven gas (NCOG
or DCOG) is used to heat the ovens in the battery.
About 40 percent of the COG (DCOG or NCOG) generated by the
battery during the coking process is underfired to the battery
3-1
-------
COAL
AIR *
COKE
/1
COKING CHAMBER
COKE BATTERY
HEATING FLUE
1(1
Y
OUTLET
STACK
CHEMICALS
1
COAL-CHEMICAL
RECOVERY
i'2
DESULFURIZATION
SULFUR RECOVERY
OTHER
PROCESSES
OTHER
PROCESSES
SAMPLING POINT
-*• SOLIDS FLOW
•-* AIR/GAS FLOW
SULFUR
Figure 3-1. Process flow diagram,
Republic Steel-Cleveland Works.
3-2
-------
along with combustion air. The products of combustion from
underfiring with coke oven gas leave the battery via the waste
gas stack. There are no add-on pollution control devices serving
the battery stack. Naturally induced stack draft, which is
regulated by dampers at the end of each flue gas canal, draws air
required for combustion through an airbox at the bottom of the
regenerator chambers.
Approximately 15 tons of coal (0.75 to 1.0 percent sulfur)
is charged through three openings in the top of each oven. A
leveling bar on the pusher machine is used to level the coal
before the coking operation begins. The coke ovens are under-
fired with coke oven gas (NCOG or DCOG), and the firing takes
place from either the coke side or the push side. More gas is
fired on the coke side of the oven since it is approximately 3
inches wider and, hence, contains more coke to heat up than the
pusher side of the oven. Heat for the coking operation is pro-
vided by a regenerative combustion system located below the
ovens. Since the combustion flue gas contains a significant
amount of process heat, two regenerators (one for combustion air
and one for combustion waste gas) are located below each oven.
Flow between the two regenerators alternates at about 30 minute
intervals as the firing of the coke ovens is reversed every 30
minutes to keep the ovens operating within the safe temperature
range of the silica refractories.
When the coking operation is complete [skin temperature of
the coke has reached 1038° to 1093°C (1900° to 2000°F)], the coke
3-3
-------
guide and quench car are moved into place, and the oven doors are
removed. The pusher then pushes the coke out of the oven through
the coke guide and into the quench car. The coke is then trans-
ported to the quench tower, where it is cooled by water sprays.
From there, it is removed to the wharf, where it is further
cooled before being conveyed to storage.
The operation of each oven is cyclic, but the battery con-
tains a sufficiently large number of ovens to maintain an essen-
tially continuous yield of byproducts. Although the time between
charging and discharge is approximately equal for all ovens,
charging times are staggered so that the flow of evolved gases
from the ovens is constant. This helps to maintain a balance of
pressure in the flues, collecting main, and battery stack.
3-4
-------
SECTION 4
SAMPLING AND ANALYTICAL PROCEDURES
Samples collected at the exit stack were analyzed for par-
ticulate, sulfur dioxide, sulfuric acid mist, and other related
pollutants. In addition, grab samples collected at the inlet and
outlet (during DCOG underfiring) of the SRU and the exit stack
were analyzed for total reduced sulfurs (TRS). This section
briefly describes the sampling and analytical procedures used in
this test; detailed descriptions of these procedures are pre-
sented in Appendix D.
4.1 SAMPLING LOCATIONS
Sampling ports were located at the 15.2-m (50-ft) level of
the 68.6-m (225-ft) outlet stack. This site is 6 stack diameters
from the nearest downstream flow disturbance and 21 stack diam-
eters from the nearest upstream flow disturbance in the 2.5-m
(8.1-ft) diameter stack (see Figure 4-1). Figure 4-2 shows the
sampling site configuration and traverse point locations. Twenty-
four points were used for velocity traverse. Particulate sam-
pling was conducted at a point of average velocity for the entire
2-hour test period.
Gaseous grab samples were collected at the inlet and outlet
of the SRU via positive pressure taps located in the connecting
ductwork.
4-1
-------
2.5 m (S.I ft) l.D.
1
68.6 m
(~225 ft)
i
i
15.2
(50
i
r
(,,
m
ft)
/
/
^
«
^
1
FLOW
r
:ID
1
\ GROUND LEVEL
Figure 4-1. Coke Battery No. 1 flue gas exit stack.
. 4-2
-------
6-in. PORT
(TRAINS 1-4)
4-in. PORT
(TRAINS 5 AND
6)
4-1n. PORT
VELOCITY TRAVERSE POINT LOCATIONS
POINT NO.
1
2
3
4
5
6
7
8
9
10
11
12
LOCATION, in.
2
6 1/2
11 1/2
17 1/4
24 3/8
34 3/4
62 3/4
73 1/8
80 3/4
86
91
95 1/2
Figure 4-2. Coke Battery No. 1 exit stack sampling site and
traverse point locations.
4-3
-------
4.2 GAS STREAM FLOW RATE, TEMPERATURE, AND COMPOSITION
Gas stream flow rate and temperature before each test series
and in conjunction with each particulate run were measured ac-
cording to the procedures described in EPA Method 2.* Velocities
were measured with an S-type pitot tube and a 0 to 0.25-inch,
inclined, draft gauge manometer. Temperatures were measured with
a calibrated thermocouple and digital potentiometer. During each
particulate test an integrated bag sample was collected, the
oxygen and carbon dioxide content was determined by Orsat analy-
sis. Method 3* sampling and analytical procedures were used in
all cases.
4.3 PARTICULATE, SULFUR DIOXIDE, AND SULFURIC ACID MIST EMISSION
TESTS
Samples were collected from a single point in the exit stack
by use of a quad train Method 5 sampling system, a standard EPA
Method 5 train, and a particulate sampling train equipped for
315°C (600°F) filter box and probe heat. Sampling was conducted
isokinetically by regulating the sampling rate relative to the
flue gas velocity. Tables 4-1 through 4-3 detail the sampling
and analytical schedules used during the NCOG and DCOG test
series. Particulate filters were glass fiber,** sample train
back halves consisted of four impingers in a Method 5 water
configuration or five impingers in a Method 8 isopropanol,
*40 CFR 60, Appendix A, Reference Methods 2 and 3, July 1980.
**
Whatman Reeve Angel 934 AH.
4-4
-------
TABLE 4-1. NCOG UNDERFIRING TEST SERIES, OCTOBER 26-30, 1981,
REVISED SAMPLING SCHEDULE
Run
No.
1
2
3
4
5
6
7
8
Sample
train No.
1.1
1.2
1.3
1.4
1.5
1.6
2.1
2.2
2.3
2.4
2.5
2.6
3.1-3.6
4.1-4.6
5.1
5.2
5.3
5.4
5.5
5.6
6.1
6.2
6.3
6.4
6.5
6.6
7.1
7.2
7.3
7.4
7.5
7.6
8.1
8.2
8.3
8.4
8.5
8.6
Probe, filter temperature,
°C
121
121
177
177
121
316
121
121
204
204
121
316
Same as
Same as
121
121
177
177
121
316
121
121
204
204
121
316
121
121
177
177
204
316
177
177
204
204
121
316
°F
250
250
350
350
250
600
250
250
400
400
250
600
Run 1
Run 2
250
250
350
350
250
600
250
250
400
400
250
600
250
250
350
350
400
600
350
350
400
400
250
600
Back-half
configuration
Method 8
Method 8
Method 8
Method 8
Method 5
Method 8
Method 8
Method 8
Method 8
Method 8
Method 5
Method 8
Same as Run 1
Same as Run 2
Method 8
Method 5
Method 8
Method 5
Method 5
Method 8
Method 8
Method 5
Method 8
Method 5
Method 5
Method 8
Method 8
Method 5
Method 8
Method 5
Method 5
Method 8
Method 8
Method 5
Method 8
Method 5
Method 8
Method 8
Note: All filters were Whatman Reeve Angel 934 AH. Sampling trains
1 through 4 operated simultaneously in quad system. During
every run, gas samples were collected at the COG inlet to the
battery and at the outlet stack for TRS and S0 analysis.
4-5
-------
TABLE 4-2. DCOG UNDERFIRING TEST SERIES, DECEMBER 6-13, 1981,
REVISED SAMPLING SCHEDULE
Run
No.
Dl
D2
D3
D4
D5
D6
Sample
train No.
1.1
1.2
1.3
1.4
1.5
1.6
2.1-2.6
3.1
3.2
3.3
3.4
3.5
3.6
4.1-4.6
5.1
5.2
5.3
5.4
5.5
5.6
6.1
6.2
6.3
6.4
6.5
6.6
Probe, filter temperature,
°C
121
121
177
177
121
316
Same as
121
121
204
204
121
316
°F
250
250
350
350
250
600
*un Dl
250
250
400
400
250
600
Same as Run D3
121
121
177
177
121
316
121
121
204
204
121
316
250
250
350
350
250
600
250
250
400
400
250
600
Back-half
configuration
Method 8
Method 8
Method 8
Method 8
Method 5
Method 8
Same as Run Dl
Method 8
Method 8
Method 8
Method 8
Method 5
Method 8
Same as Run D3
Method 8
Method 5
Method 8
Method 5
Method 5
Method 8
Method 8
Method 5
Method 8
Method 5
Method 5
Method 8
Note: All filters were Whatman Reeve Angel 934 AH. Sample trains
1 through 6 operated simultaneously. Gas samples were
collected during every run at the inlet and outlet of the
desulfurization unit and"at the outlet stack for TRS and SC2
analysis.
4-6
-------
TABLE 4-3. NCOG AND DCOG UNDERFIRING TEST SERIES ANALYTICAL SCHEDULE
Run
1,3,
01,02
Sampl Ing
train
Method 5 with
Method 8 back
half
Method 5 with
Method 8 back
half
Method 5 with
Method 8 back
half
Method 5 with
Method 8 back
half
Method 5 with
H20 in the
impingers
Filter
1.0. No.
1.1
3.1
Dl.l
02. 1
1.2
3.2
01.2
02.2
1.3
3.3
01.3
02. 3
1.4
3.4
01.4
02.4
1.5
3.5
01.2
02.5
Probe and filter
temperature,
°C
121
121
177
177
121
°F
250
250
350
350
250
Laboratory protocol
Front half8
1. Desiccate and weigh
2. IPA-rlnse and titrate
3. H20-r1nse and titrate
1. Desiccate and weigh
2. Heat 2 h at 177°C (350°F)
3. Reweigh
4. IPA-rinse and titrate
5. H20-rinse and titrate
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H,0-rinse and titrate
c
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H-0-rlnse and titrate
2
1. Desiccate and weigh
2. Divide filter, desic-
cate and weigh
3. a. Heat 2 h at 177°C (350°F),
heat 4 h at 177°C (350°F),
heat 2 h at 204°C (400°F),
heat 4 h at 204°C (400°F),
heat 2 h at 316°C (600°F),
IPA-rinse and titrate,
H20-rinse and titrate
Back half
Standard Method 8
Standard Method 8
Standard Method 8
Standard Method 8
1. TOCb r
2. E-C ext.
(continued)
-------
TABLE 4-3 (continued)
i
00
Run
2,4.
D3.D4
Sampl Ing
train
CCS filter
holder with
Method 8
back half
Method 5 with
Method 8 back
half
Method 5 with
Method 8 back
half
Method 5 with
Method 8 back
half
Method 5 with
Method 8 back
half
Filter
1.0. No.
1.6
3.6
01. 6
02.6
2.1
4.1
03. 1
04. 1
2.2
4.2
03.2
04.2
2.3
4.3
03. 3
04.3
2.4
4.4
03.4
Probe and filter
temperature,
°C
316
121
121
204
204
°F
600
250
250
400
400
Laboratory protocol
Front half3
b. 121°C (250°F) ~ TOC
temperature profile
- 316°C (600°F)
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H,0-r1nse and titrate
t
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H,0-rinse and titrate
2
1. Desiccate and weigh
2. Heat 2 h at 204°C (400°F)
3. Reweigh
4. IPA-rinse and titrate
5. H-O-rinse and titrate
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H00-rinse and titrate
L.
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H-O-rinse and titrate
Back-half
Standard Method 8
Standard Method 8
Standard Method 8
Standard Method 8
Standard Method 8
(continued)
-------
TABLE 4-3 (continued)
Run
5.D5
Sampl 1ng
train
Method 5 with
H20 In the
Implngers
CCS filter
holder with
Method 8 back
half
Method 5 with
Method 8 back
half
Method 5 with
H20 In the
Implngers
Method 5 with
Method 8 back
half
Filter
I.D. No.
2.5
4.5
03. 5
04. 5
2.6
4.6
03. 6
04. 6
5.1
05. 1
5.2
05. 2
5.3
05.3
Probe and filter
temperature,
°c
121
316
121
121
177
°F
250
600
250
250
350
Laboratory protocol
Front half3
1. Desiccate and weigh
2. Divide filter, desic-
cate and weigh
3. a. Heat 2 h at 177°C (350°F),
heat 4 h at 177°C (350°F),
heat 2 h at 204°C (400°F),
heat 4 h at 204°C (400°F),
heat 2 h at 316°C (600°F),
IPA-rlnse and titrate,
H20-rinse and titrate
b. 121°C (250°F) - TOC
temperature profile
- 316°C (600°F)
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H,0-rinse and titrate
c.
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H-O-rinse and titrate
1. Desiccate and weigh
2. Heat 2 h at 177°C (350°F)
3. Reweigh
4. IPA-rinse and titrate
5. H-0-rlnse and titrate
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H-0-rinse and titrate
Back half
1. TOCb r
2. E-C ext.c
Standard Method 8
Standard Method 8
1. TOCb c
2. E-C ext.
Standard Method 8
(continued)
-------
TABLE 4-3 (continued)
Run
6,06
Sampling
train
Method 5 with
H20 In the
Implngers
Method 5 with
H20 In the
Implngers
CCS filter
holder with
Method 8
back half
Method 5 with
Method 8 back
half
Method 5 with
HzO 1n the
Implngers
Filter
I.D. No.
5.4
05.4
5.5
05. 5
5.6
D5.6
6.1
06. 1
6.2
06.2
Probe and filter
temperature,
°C
177
121
316
121
121
°F
350
250
600
250
250
Laboratory protocol
Front half3
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H20-rinse and titrate
1. Desiccate and weigh
2. Divide filter, desic-
cate and weigh
3. a. Heat 2 h at 177°C (350°F),
heat 4 h at 177°C (350°F),
heat 2 h at 204°C (400°F),
heat 4 h at 204°C (400°F),
heat 2 h at 316°C (600°F),
IPA-rinse and titrate,
HzO-rinse and titrate
b. 121 °C (250°F) - TOC
temperature profile
- 316°C (600°F)
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H,0-rinse and titrate
f.
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H20-rinse and titrate
1. Desiccate and weigh
2. Heat 2 h at 204°C (400°F)
3. Reweigh
4. IPA-rinse and titrate
5. H.O-rlnse and titrate
Back half
1. TOCb p
2. E-C ext.
1 . TOCb
2. E-C ext.
Standard Method 8
Standard Method 8
1. TOCb r
2. E-C ext.
(continued)
-------
TABLE 4-3 (continued)
Run
7
Sampling
train
Method 5 with
Method 8 back
half
Method 5 with
H20 In the
impingers
Method 5 with
H20 in the
Impingers
CCS filter
holder with
Method 8
back half
Method 5 with
Method 8 back
half
Filter
I.D. No.
6.3
06.3
6.4
06. 4
6.5
06.5
6.6
06. 6
7.1
Probe and filter
temperature,
°C
204
204
121
316
121
°F
400
400
250
600
250
Laboratory protocol
Front halfa
1. Desiccate and weigh
2. IPA-rlnse and titrate
3. H~0-rinse and titrate
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H20-r1nse and titrate
1. Desiccate and weigh
2. Divide filter, desic-
cate and weigh
3. a. Heat 2 h at 177°C (350°F),
heat 4 h at 177°C (350°F),
heat 2 h at 204 °C (400°F),
heat 4 h at 204°C (400°F),
heat 2 h at 316°C (600°F),
IPA-rinse and titrate,
H20-rinse and titrate
b. 121°C (250°F) *• TOC
temperature profile
+ 316°C (600°F)
1. Desiccate and weigh
2. IPA-rinse and titrate
3. H_0-r1nse and titrate
£
1. Desiccate and weigh
2. Hold
Back half
Standard Method 8
1. TOCb r
2. E-C ext.
1. TOCb r
2. E-C ext.c
Standard Method 8
Hold
(continued)
-------
TABLE 4-3 (continued)
I
M
to
(continued)
Run
8
Sampling
train
Method 5 with
H20 in the
impingers
Method 5 with
Method 8 back
half
Method 5 with
HzO in the
impingers
Method 5 with
H20 in the
impingers
CCS filter
holder with
Method 8
back half
Method 5 with
Method 8 back
half
Method 5 with
H20 1n the
impingers
Method 5 with
Method 8 back
half
Filter
I.D. No.
7.2
7.3
7.4
7.5
7.6
8.1
8.2
8.3
Probe and filter
temperature,
°C
121
177
177
204
316
177
177
204
°F
250
350
350
400
600
350
350
400
Laboratory protocol
Front half3
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Hold
Back half
Hold
Hold
Hold
Hold
Hold
Hold
Hold
Hold
-------
TABLE 4-3 (continued)
*»
i
M
10
Run
Sampling
train
Method 5 with
H20 1n the
Implngers
Method 5 with
Method 8 back
half
CCS filter
holder with
Method 8
back half
Filter
1.0. No.
8.4
8.5
8.6
Probe and filter
temperature,
°C
204
121
316
°F
400
250
600
Laboratory protocol
Front half3
1. Desiccate and weigh
2. Hold
1. Desiccate and weigh
2. Heat 2 h at 135°C (275°F),
heat 4 h at 135°C (275°F),
heat 2 h at 149°C (300°F),
heat 4 h at 149°C (300°F),
heat 2 h at 163°C (325°F),
heat 4 h at 163°C (325°F),
heat 2 h at 177°C (350°F),
heat 4 h at 177°C (350°F),
heat 2 h at 204°C (400°F),
heat 4 h at 204°C (400°F),
heat 2 h at 316°C (600°F),
IPA-rlnse and titrate.
HpO-Mnse and titrate
1. Desiccate and weigh
2. Hold
Back half
Hold
Hold
Hold
aFront half filter catches were saved after their analysis.
Total organic carbon.
Ether-chloroform extraction.
-------
hydrogen peroxide configuration. Stack, probe, filter, and
impinger gas temperatures were monitored for each train during
sampling.
After sampling was completed, filters were removed and
placed in a petri dish. The nozzle, probe, and filter holder
portions of the sample train were then acetone-rinsed. The
acetone rinse and particulate caught on the filter media were
dried at room temperature, desiccated to a constant weight, and
weighed on an analytical balance. Total filterable particulate
matter was determined by adding these two values. Selected
filters were heated at indicated temperatures for 2 to 4 hours,
desiccated to a constant weight, and weighed on an analytical
balance. After the indicated heat treatment, the filterable
particulate matter content was determined by adding these two
values.
Acid sulfate and water-soluble sulfates were determined by
washing the particulate catch samples sequentially with IPA and
distilled water, and titrating the eluates with barium perchlo-
rate.
Total organic carbon was determined from selected filters by
heating to the indicated temperature in the presence of a leak-
free nitrogen purge. After the purge gas had been diluted and
oxidized, it was collected in a stainless steel tank. An aliquot
was injected into a gas chromatograph with oxidation-reduction
capabilities.
Sulfuric acid mist and sulfur dioxide concentrations were
determined from the sampling trains with Methods 8 back halves.
4-14
-------
The first and second impingers contained the acid mist sample,
and the third and fourth impingers contained the SO- sample. In
each case, the concentrations were determined by titrating with
barium perchlorate.
The Method 5 impinger contents for selected samples were
treated by an ether-chloroform extraction technique to determine
organic and inorganic condensibles. The respective extracts were
placed in tared beakers and evaporated to dryness. The organic
fraction was dried at ambient temperature, and the inorganic
fraction, at 105°C (221°F). The beakers were then desiccated to
a constant weight and weighed to the nearest 0.1 mg. Condensible
total organic carbon also was determined, by subjecting an ali-
quot of Method 5 back-half water to the ampule technqiue of
organic oxidation. This method involves heating the aliquot in a
carbon-free atmosphere in the presence of a catalyst and quanti-
tatively determining carbon dioxide.
4.4 REDUCED-SULFUR EMISSION TESTS
Gas samples were analyzed for reduced-sulfur compounds (H-S,
COS, and CS2) and SO- by gas chromatographic (GC) separation and
j^
flame photometric detection (FPD). Fifteen-liter Tedlar bags
were filled with COG via positive-pressure taps located in the
ductwork at the inlet and outlet of the SRU or filled with exit
stack gas by a leak-free Teflon diaphragm pump. Only Teflon
tubing and connections were used during sample collection. Inlet
and outlet SRU samples were collected simultaneously.
4-15
-------
A sample aliquot was taken for analysis by a sample loop and
multiport valve system. Aliquot size was determined by the
sample loop size. For separation of the reduced-sulfur and
sulfur dioxide components, the sample aliquot was passed through
various chromatographic columns. Flow through the sample loop
and columns was controlled by electronic integration. After
separation, the relative quantity of each component was measured
as the electrical potential (yV-s) produced from the flame photo-
metric detector and measured by the integrator. Component cali-
bration curves of response versus concentration were made daily
by permeation devices and dynamic dilution. The FPD response was
determined to be linear from 0 to 70 ppm. Samples with component
concentrations greater than 70 ppm were analyzed in the FPD
linear range by reducing the sample loop size. Audit and stan-
dard gases were diluted dynamically before they entered the
sample loop. Harmon Engineering and Testing of Auburn, Alabama,
provided an onsite GC-FPD analysis.
Appendix D presents a complete description of the sampling
and analytical procedures used. Appendix A presents calcula-
tions, including gas velocity data. Appendices B and C present
field and laboratory data sheets, and Appendix E describes the
equipment calibration procedures and results.
4-16
-------
SECTION 5
QUALITY ASSURANCE
Because the end product of testing is the production of
representative emission results, quality assurance is one of the
primary facets of stack sampling. Quality assurance guidelines
outline what is pertinent to the production of acceptable data
and emission data are considered reliable only if the proper
quality assurance measures are taken. The steps outlined herein
are intended to ensure the production of quality data through our
testing and analysis procedures.
Quality control procedures for the standard reference
methods were used throughout this test series. These included,
but were not limited to, the following:
0 Calibration of field sampling equipment. Tables 5-1
through 5-12 summarize calibration of equipment used in
this test series. Calibration guidelines are described
in more detail in Appendix E.
0 Train configuration and calculation checks.
0 Onsite quality assurance checks such as leak checks of
the sampling train, the pitot tube, and the Orsat line.
0 Use of designated analytical equipment and sampling
reagents.
0 Lab analysis procedures. Tables 5-13 and 5-14 show the
results of quality assurance tests for accuracy of the
analysis of field samples.
5-1
-------
TABLE 5-1. FIELD EQUIPMENT CALIBRATION, QUAD TRAIN NO. 1 (NCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-2
1001
125
174
C02
231 02
CO
194
271
Inlet
Outlet
1
2-1
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Caliper
Allowable
deviation
Y +0.02 Y
AH G» +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.52
1.5S
(+2r, saturated)
+0.5X
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-3.0%
OK
+0.3%
0.4%
+0.2%
+0.1%
-0.4%
OK
+0.1 g
+0.02
in.
-2°F
-1°F
0.001 in.
0.002 in.
Within
allowable
limits
/
/
/
/
/
'
/
/
/
/
^
Comments
in
-------
TABLE 5-2. FIELD EQUIPMENT CALIBRATION, QUAD TRAIN NO. 2 (NCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-10
1001
125
174
C00
w •
231 D£
194
271
Inlet
Outlet
2
2-2
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Cali per
Allowable
deviation
Y +0.02 Y
AH P +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1.5%
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-3.1%
OK
+0.3%
0.4%
+0.2%
+0.15
-0.4%
OK
+0.1 g
+0.02 in.
-2°F
-1°F
0.001 in
0.002 in
Within
allowable
limits
/
/
/
/
•
*
/
/
'
/
/.
/
^
Comments
Ul
I
U)
-------
TABLE 5-3. FIELD EQUIPMENT CALIBRATION, QUAD TRAIN NO. 3 (NCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-1
1001
124
174
CO?
231 o?
CO
194
271
Inlet
Outlet
3
3-3
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Cali per
Allowable
deviation
Y +0.02 Y
AH (a +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1 5%
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-2.2%
OK
-0.4%
0.4%
+0.2%
+0.1%
-0.4%
OK
+0.1 g
+0.02 in.
0°F
0.001 in.
0.000 in.
Within
allowable
limits
'
'
/
/
/
'
J
^
Comments
Ul
I
*>.
-------
TABLE 5-4. FIELD EQUIPMENT CALIBRATION, QUAD TRAIN NO. 4 (NCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-5
1001
124
174
C09
231 0~
CO
194
271
Inlet
Outl et
4
3-4
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F or 3F
Caliper
Allowable
deviation
Y +0.02 Y
AH 0 +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1.5%
(^2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-3.6%
OK
-0.4%
0.4%
+0.2%
+0.1%
-0.4%
OK
+0.1 g
+0.02 in.
0°F
-1°F
0.000 in.
0.003 in.
Within
allowable
limits
/
/
/
/
/
J
*
/
'
/
/
^
Comments
01
I
Ul
-------
TABLE 5-5. FIELD EQUIPMENT CALIBRATION, TRAIN NO. 5 (NCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-4
186
207
203
C02
231 Op
CO
194
271
Inlet
Outlet
6-105
6-114
8-103
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Caliper
Allowable
deviation
Y +0.02 Y
AH (a +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1.5S
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-0.6%
0.00
-0.4%
0.3%
+0.2%
+0.1%
-0.4%
OK
+0.1 g
+0.02 in.
-3°F
+1 °F
Q.'QOQ in.'
n nfll -in
\J f \J\S t Ilia
Within
allowable
limits
/
/
/
/
/
/
/
/
*
/
y
Comments
-------
TABLE 5-6. FIELD EQUIPMENT CALIBRATION, TRAIN NO. 6 (NCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-8
186
207
203
C02
231 02
CO
194
271
Inlet
Outlet
A
B
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Cali per
Allowable
deviation
Y +0.02 Y
AH (3 +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1.5%
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
On +0.004 in.
Actual
deviation
-0.4%
0.00
-0.4%
0.3%
t f\ OO/
+0.2%
+01%
1 \J • 1/0
-0.4%
OK
+0.1 g
+0.02 in,
+2°F
-3°F
0.001 in.
0.001 in.
Within
allowable
limits
/
/
/
/
,
/
'
/
/
/
/
/
/
/
Comments
en
-------
TABLE 5-7. FIELD EQUIPMENT CALIBRATION, QUAD TRAIN NO. 1 (DC06)
Equipment
Meter box
Pi tot tube
Digital
Indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-2
1001
125
133
C09
230 0~
or
1
196
225
Inlet
Outlet
1-1
2-1
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Cali per
Allowable
deviation
Y +0.02 Y
AH 0 +0.15
(Y +0.05 Y post- test)
Cp +0.01
0.5%
1.5%
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-2.7%
OK
+0.3%
-0.5%
+0.4%
-0.3%
-0.5%
-4°F
+0.3 g
+0.01 in.
+4°F
+2°F
0.001 in.
0.001 in.
Within
allowable
limits
/
'
'
J
/
'
/
'
Comments
Correction factor used
in
I
oo
-------
TABLE 5-8. FIELD EQUIPMENT CALIBRATION, QUAD TRAIN NO. 2 (DC06)
Equipment
Meter box
PUot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-5
1001
125
133
C02
230 09
CO^
2
196
225
Inlet
Outlet
1-2
2-2
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Cali per
Allowable
deviation
Y +0.02 Y
AH 9 +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1.5%
(+2% saturated)
+0.5%
+2°F
+J).5 g
+0.10 in. Hrj.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-2.3%
OK
+0.3%
-0.5%
+0.4%
-0.3%
-0.5%
-4°F
+ 0.3 q
+0.01 in.
+4°F
+2°F
0.001 in.
0.000 in.
Within
allowable
limits
/
/
/
/
/
/
/
/
/
/
/
/
Comments
Correction factor used
en
I
vo
-------
TABLE 5-9. FIELD EQUfPMENT CALIBRATION, QUAD TRAIN NO. 3 (DCOG)
Equipment
Meter box
PHot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-8
1001
124
133
C0?
230 0,
or
3
196
225
Inlet
Outlet
1-3
2-3
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Caliper
Allowable
deviation
Y +0.02 Y
AH P +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
i.sr,
(+2% saturated)
+0.5%
+2°F
+.0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-0.6*
OK
-0.5%
-0.5%
+0.4%
-0.3%
-0.5%
-2°F
+0.3 g
+0.01 in.
-3°F
-2°F
0.000 in.
0.001 in.
Within
allowable
limits
/
/
/
/
/
/
/
/
/
/
•
/
/
Comments
Ul
-------
TABLE 5-10. FIELD EQUIPMENT CALIBRATION, QUAD TRAIN NO. 4 (DCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-4
1001
124
133
C09
230 0^
CO
4
196
225
Inlet
Outlet
1-4
2-4
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F of 3F
Caliper
Allowable
deviation
Y +0.02 Y
AH (? +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1.5%
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
+0.9%
OK
-0.5%
-0.5%
+0.4%
-0.3%
-0.5%
0°F
+0.3 g
+0.01 in.
0°F
0°F
3.001 in.
0.001 in.
Within
allowable
limits
/
/
/
/
/
/
/
/
/
/
/
/
/
/
Comments
I
en
l
-------
TABLE 5-11. FIELD EQUIPMENT CALIBRATION, TRAIN NO. 5 (DCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-1
034
221
133
C09
230 Oo
CO
5
196
225
Inlet
Outlet
352-104
7-101
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Caliper
Allowable
deviation
Y +0.02 Y
AH (3 +0.15
(Y +0.05 Y post-test)
Cp +0.01
0.5%
1.5%
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-3.7%
0.00
+0.4%
-0.5%
+0.4%
-0.3%
Oc o/
. 5%
OK
+0.3 g
+0.01 in.
-2°F
-5°F
0.002 in.
0.002 in.
Within
allowable
limits
/
/
/
/
J
*
/
'
/
^
Comments
Ui
H
ro
-------
TABLE 5-12. FIELD EQUIPMENT CALIBRATION, TRAIN NO. 6 (DCOG)
Equipment
Meter box
Pi tot tube
Digital
indicator
Thermocouples
and stack
thermometers
Orsat analyzer
Impinger
thermometer
Trip balance
Barometer
Dry gas
thermometer
Probe nozzle
I.D.
No.
FB-6
034
221
133
CO-
230 0~
or
6
196
225
Inlet
Outlet
6-108
6-105
Calibrated
against
Wet test meter
Standard pi tot
tube
Millivolt signals
ASTM-2F or 3F
Standard gas
ASTM-2F or 3F
Type S weights
NBS traceable
barometer
ASTM-2F Of 3F
Caliper
Allowable
deviation
Y +0.02 Y
AH (3 +0.15
(Y +0.05 Y post- test)
Cp +0.01
0.5%
1.5?,
(+2% saturated)
+0.5%
+2°F
+0.5 g
+0.10 in. Hg.
(0.20 post test)
+5°F
Dn +0.004 in.
Actual
deviation
-1.6%
0.00
+0.4%
-0.5%
+0.4%
-0.3%
-0.5%
OK
\Jt\
+0.3 g
+0.01 in.
-4°F
-4°F
0.001 in.
0.000 in.
Within
allowable
limits
/
/
/
/
/
/
/
^
/
/
/
^
/
/
Comments
•
U>
-------
TABLE 5-13. FILTER AND REAGENT BLANK ANALYSIS, NCOG TEST SERIES
Sample type and
analytical procedure
Acetone
Gravimetric
IPA extraction
H20 extraction
Filter
Gravimetric
IPA extraction
H20 extraction
Total organic carbon
(oxidation tech-
nique)
Method 5 back half
Ether/chloriform
Inorganic
Organic
Total organic carbon
(ampute tech-
nique)
Method 8 IPA solution
H2S04 titration
Method 8 H20^ solution
S02 titration
Lab No. (sample
volume, ml)
CB 954 (219)
CB 955 (348)
CB 954
CB 954
CB 894
CB 895
CB 900
CB 901
CB 901
CB 901
CB 900
CC 026 (196)
CC 027 (384)
CC 026 (150)
CC 027 (150)
CC 026 (60)
CC 027 (60)
CB 982
CB 983
CB 984
CB 985
CC 013-15
Blank weight,
mg
0.4
0.7
<0.3
<0.21
0.3
0.8
0.3
0.7
<0.3
<0.42
1.28
4.0
3.8
1.6
1.3
0.5
0.05
0.25
0.22
0.20
<0.15
<1
Comments
0.01 used in
calculations
5-14
-------
TABLE 5-14. FILTER AND REAGENT BLANK ANALYSIS, DCOG TEST SERIES
Sample type and
analytical procedure
Acetone
Gravimetric
IPA extraction
HpO extraction
Filter
Gravimetric
IPA extraction
H20 extraction
Total organic carbon
(oxidation tech-
nique)
Method 5 back half
Ether/chloriform
Inorganic
Organic
Total organic carbon
(ampute technique)
Method 8 IPA solution
H2S04 titration
Method 8 H202 solution
S02 titration
Lab No. (sample
volume, ml)
CC 769 (270)
CC 770 (275)
CC 769
CC 769
CC 666
CC 672
CC 671
CC 673
CC 669
CC 669
CC 666
CC 666
CC 771 (225)
CC 772 (205)
CC 771 (150)
CC 772 (150)
CC 771 (60)
CC 772 (60
773-6
CC 778-9
Blank weight,
mg
-0.9
1.1
<0.05
<0.24
0.2
0.1
0.3
0.2
<0.3
<0.24
1.58
1.65
-0.9
-0.5
4.7
-0.3
0.3
0.7
<0.11
0.0
Comments
0.0 used in cal-
culation
0.0 used in cal-
culations
0.0 used in cal-
culations
0.01 used in cal-
. culations
0.0 used in cal-
culations
5-15
-------
0 Internal and external audits to ensure accuracy in
sampling and and analysis. Onsite audit data sheets
are included in Appendix B, Section 1.1 and 2.1.
Audit solutions prepared by EPA were used to check the
analytical procedures and reagents prior to onsite S02 sample
analysis. The results of the onsite analytical audit are pre-
sented below:
Audit solution Measured
Audit sample concentration, concentration, Percent
lot No. mg/dNm mg/dNm difference
3291 (NCOG) 22.89 22.75 -0.6
3575 (NCOG) 17.16 16.98 -1.0
8026 (DCOG) 381.3 383.3 +0.5
6220 (DCOG) 1334.6 1321.2 -1.0
Table 5-15 details the results obtained by Method 15 analy-
sis of EPA-prepared reduced-sulfur gases.
Sampling equipment, reagents, and analytical procedures for
this test series follow and meet all necessary guidelines set
forth for accurate test results. Calibrations of particulate
sampling equipment are all within limits described for Method 5
in the Federal Register.* Sample analysis and reagent quality
also meet with Federal regulations described in Method 5 of the
Federal Register.*
40 CFR 60, Appendix A, Reference Method 5, July 1, 1980.
5-16
-------
TABLE 5-15. SUMMARY OF RESULTS OBTAINED THROUGH METHOD 15
ANALYSIS OF AUDIT GASES3
Cylinder
I.D.
RTI-b-704
428 ppm H2S
RTI-705
649 ppm H0S
L.
RTI-1584
100 ppm COS
Date
1/26/82
12/8/81
12/9/81
12/9/81
12/9/81
12/12/81
Time
1400
1754
1730
1648
1757
1530
TRS concentra-
tion, ppm
449
797
540
94
103
96
Comments
Dynamic dilution
Bag sample
Dynamic dilution
35.1 to 1
Bag sample
Dynamic dilution
3.18 to 1
Bag sample
All acceptable COS results required a correction factor of 1.257 because of
an incorrect permeation rate.
3RTI = Research Triangle Institute.
5-17
-------
APPENDIX A
COMPUTER PRINTOUTS AND EXAMPLE CALCULATIONS
A-l
-------
CONCENTRATION CALCULATIONS
CS (Part), mg/m3 = MN/V (m3)
mstd
CS (Part), gr/dscf = 0.001 x MN x 15.43/Vm (ft3)
mstd
CS (S09 or H,SOA), mg/m3 = SN/Vm (m3)
i *• * mstd
CS (S02 or H2S04), ppm = CS (S02 or H2S04), mg/m3 x 24.06/MW
CS (SO, or H9SOJ, gr/dscf = 0.001 x SN x 15.43/V (ft3)
* ^ 4 mstd
where
CS (Part) = concentration of participate at stated parameters
CS (SOp) = concentration of sulfur dioxide at stated parameters
MN = particulate catch at stated parameter (mg)
V = volume method at 68°F and 29.92 in.Hg, (m3 or ft3)
mstd
SN = sulfur dioxide catch (mg) or sulfuric acid catch (mg)
MW = molecular weight of S09 = 64 g/g mole, H9SO,, = 98,
H2S04-2H20 = 134 L *• *
A-2
-------
1.0 NCOG Underfiring Test Series
October 1981
A-3
-------
STACK VELOCITY DATA
PLANT
DATE
SAMPLING LOCATION
RUN NUMBER
CLOCK TIME
OPERATOR
AMBIENT TEMP. (OEG.F)
BAR.PRESS.(IN HG)
STATIC PRESS.(IN H20)
MOLECULAR HEIGHT
STACK INSIDE OIM(IN)
PITOT TUBE COEFF.
MOISTURE CONTENT(X)
TRAVERSE
POINT
NO.
POSITION
INCHES
REPUBLIC STEEL CLEVELAND
io/22/ei
COKE BATTERY STACK-NO.1
PRE-1
954
CB-DO
54.
29.60
-1.20
29.00
97.500
.80
12.00
VELOCITY
HEAO
(IN H20)
STACK
TEMP
(OEG.F)
01
02
03
OQ
05
Ob
07
08
09
10
11
12
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.020
.050
.045
.060
.000
.OBO
.070
.060
.050
.070
.060
.050
128.
305.
430.
510.
480.
406.
487.
492.
497.
496.
497.
497.
AVERAGE
.058
442.
-------
PLANT
DATE
SAMPLING LOCATION
RUN NUMHER
STACK AREA, SO. FT.
STACK ABS. PRES.. IN HG.
STACK CAS TEMPERATURCt OEG.F
3URUVEL HO X STACK TEMP ABS)
REPUBLIC STEEL CLEVELAND
10/28/81
CUKE BATTERY STACK-NO.1
PRE-1
51.809
29.51
• 02.
7.2
STACK GAS VELOCITY, ACT. FPS 17.6
STACK GAS VOLUME (MET), ACT. CFM. 50876.8
STACK GAS VOLUME (ORY), ACT. CFM. aB291.5
STACK GAS VOLUME 3 29.92 IN. HG AND 68 DG.
(DRY) 27879.9
(WET) 31681.H
F !
\
t_n
-------
SAMPLE CALCULATIONS
SYMBOLS!
AREA CROSS-SECTIONAL STACK AREA, SO FT
BPRES BAROMETRIC PRESSURE, IN HG
OELP DELTA P
OIA DIAMETER OF CIRCULAR STACK, IN
DIM1 LENGTH OF RECTANGULAR STACK, IN
DIM2 WIDTH OF RECTANGULAR STACK, IN
MOIST MOISTURE CONTENT
M*» MOLECULAR WEIGHT
NP NUMBER OF TRAVERSE POINTS
BM MOLE FRACTION WATER VAPOR
PTC PITOT TUBE COEFFICENT
SPUES STATIC PRESSURE, IN H20
STEMP STACK TEMPERATURE, OEG F
STPRES STACK PRESSURE, IN HG
STVEL STACK VELOCITY, AFPM
TEI*P TEMPERATURE, DEC F
VH VELOCITY HEAD, IN H?O
SVOLFLH STANDARD VOLUMETRIC FLOM (WET), ACFM
VOLFLW VOLUMETRIC FLOW (WET), ACFM
SVOLFLO STANDARD VOLUMETRIC FLOW (DRY), DSCFM
FORMULAS AND SAMPLE CALCULATIONS:
SUMI30RTIVH * TEMP)) 86.2
DEL? = — -— — = = 7.2
NP 12
STPRES = BPKES + (SPRES/13.6) = 29.60 * ( -1.20/13.6) = 29.5 IN HG
SUM (STEMP] 5305.
StEMP = — r • — — a 442. DEC F
NP 12
3.1016 * (DIA/2)**2 3.1416 * ( 97.500/2)**2
AREA(CIRCULAR STACK) = — = — « 51.849 SO FT
104 144
85.49 * PTC • DELP 85.49 * .84 • 7.2
STVEL « " ———-—— = ...... z 17.6 AFPM
SORT(MH • STPRF31 SORT( 29.00 • 29.5 )
VOLFLW a 60. » STVEL * AREA = 60. * 17.6 * 51.849 = 54876.8 ACFM
SVOLFLM * VOLFLM * STPRES * ( 460. + 68. ) 54876.8 * 29.5 * ( 460. * 68. )
................................ s ........—................... .. s 31681.8 ACFM
29.92 * ( STEMP » 460. ) 29.92 * ( 442.1 » 460. )
3VOLFLD = SVOLFLW * (1 - BH) f 31681.8 * (1 - .12) s 27879.9 DSCFM
-------
STACK VELOCITY DATA
I
-J
PLANT
DATE
SAMPLING LOCATION
RUN NUMBER
REPUBLIC STEEL CLEVELAND
10/22/81
COKE BATTERY STACK-NO.1
PRE-2
CLOCK TIME 95Q
OPERATOR CB-00
AMBIENT TEMP. (DEG.F) 54.
BAR. PRESS. (IN H9) 29.60
STATIC PRESS. (IN H20) -1.20
MOLECULAR WEIGHT 29.00
STACK INSIDE DIM(IN) 97.500
PITOT TUBE COEFF. .84
MOISTURE CONTENTU) 12.00
TRAVERSE POSITION
POINT INCHES
NO.
01 .0
_. 02 ..-. ^0
03 .0
04 .0
05 .0
06 .0
07 .0
08 .0
09 .0
10 .0
11 .0
12 .0
VELOCITY
HEAD
(IN H20)
.045
.050
.060
.060
.060
.060
.060
.055
.050
.050
.040
.040
STACK
TEMP
(DEG.F)
345.
392.
415.
430.
452.
473.
480.
483.
484.
486.
487.
487.
AVERAGE
.052
451,
-------
PLANT
0»TC
SAMPLING LOCATION
RUN NUMBER
STACK AREA, SO. FT.
STACK ABS. PRES., IN H6.
STACK GAS TEMPERATURE, DEG.F
SQRMVEL HD X STACK TEMP ABS)
REPUBLIC STEEL CLEVELAND
10/22/81
COKE BATTERY STACK-NO.1
PRE-2
51.8«9
a*.si
051.
6.9
STACK 6AS VELOCITY, ACT. FPS 16.9
STACK GAS VOLUME (NET), ACT. CFM. 52657.0
STACK GAS VOLUME (DRY), ACT. CFM. 46336.2
STACK GAS VOLUME 3 29.92 IN. HG AND 66 DG. F
(DRY) 26485.5
(WET) 30097.2
I
oo
-------
SAMPLE CALCULATIONS
SYMBOLS:
AREA CROSS-SECTIONAL STACK AREA, SO FT
BPRES BAROMETRIC PRESSURE, IN HG
OELP DELTA P
DIA DIAMETER OF CIRCULAR STACK, IN
OIMJ LENGTH OF RECTANGULAR STACK, IN
DIM2 WIDTH OF RECTANGULAR STACK, IN
MOIST MOISTURE CONTENT
MM MOLECULAR WEIGHT
NP NUMBER OF TRAVERSE POINTS
BN MOLE FRACTION MATER VAPOR
PTC PITOT TUBE COEFF1CENT
SPRES STATIC PRESSURE, IN H20
STEMP STACK TEMPERATURE, DEC F
STPRES STACK PRESSURE, IN HG
STVEL STACK VELOCITY, AFPM
TEMP TEMPERATURE, DEC F
VH VELOCITY HEAD, IN M20
SVOLFLM STANDARD VOLUMETRIC FLOW (WET), ACFM
VOLFLW VOLUMETRIC FLO* (WET), ACFM
SVOLFLD STANDARD VOLUMETRIC FLOW (DRY), DSCFM
I
vo
FORMULAS AND SAMPLE CALCULATIONS:
SUM(SORT(VM * TEMP)! 82.7
6ELP « ———————— e .......... . 6.9
NP 12
STPRES s BPRES * (SPRES/13.6) « 29.60 » ( -1.20/13.6) * 29.5 IN HG
SUMISTEMP) 5414.
"~~ SfEMP s ———— • .—.—— s 451. DEC F
NP 12
3.1416 * (DlA/2)**2 3.1416 * ( 97.500/2)0*2
AREA(CIRCULAR STACK) a ...——— = . a 51.849 SO FT
144 144
65.49 • PTC * DELP 05.49 • .84 * 6.9
STVEL « ..—.—.—— • — ............... s 16.9 AFPM
SORT [MW * STPRES) SORT { 29.00 » 29.5 )
VOLFLW s 60- • STVEL * AREA e 60. • 16.9 • 51.849 « 52657.0 ACFM
SVOLFLW c VOLFLW * STPRES • ( 460. * 68. ) 52657.0 * 29.5 • ( 460. * 68. )
......... ............... .. * ........ ................ .. * 30097.2 ACFM
29.92 • ( STEMP * 460. ) 29.92 * ( 451.2 « 460. )
SVOLFLO e SVOLFLW • (I - BW) s 30097.2 » (1 - .12) « 26485.5 OSCFM
-------
STACK VELOCITY DATA
PLANT
DATE
SAMPLING LOCATION
RUN NUMBER
CLOCK TIME
OPERATOR
AMBIENT TEMP. (DEG.F)
BAR.PRESS.(IN HC)
STATIC PRESS.(IN H20)
MOLECULAR HEIGHT
STACK INSIDE DIM(IN)
PITOT TUBE COEFF.
MOISTURE CONTENT(X)
TRAVERSE
POINT
NO.
POSITION
INCHES
REPUBLIC STEEL CLEVELAND
10/27/61
COKE STACK
V.T.
1300
DO/HP
62.
29.39
•1.20
29.00
97.500
.63
12.00
VELOCITY
HEAD
(IN H20)
STACK
TEMP
(DEG.F)
>
I
01
02
03
04
05
06
07
06
09
10
11
12
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.042
.050
.005
.060
.055
.056
.065
.065
.064
.062
• 060
.055
445.
464.
476.
494.
515.
515.
512.
511.
510.
509.
507.
507.
AVERAQT
,057
-------
PLANT
DATE
SAMPLING LOCATION
RUN NUMBER
STACK AREA, SO. FT.
STACK ABS. PRE3.. IN HC.
STACK GAS TEMPERATURE* DEG.F
SQRT(VEL HD X STACK TEMP ABS)
REPUBLIC STEEL CLEVELAND
10/27/81
COKE STACK
V.T.
SI.649
29.30
499.
T.4
STACK GAS VELOCITY, ACT. FPS 1S.O
STACK GAS VOLUME (MET), ACT. CFM. 56014.3
STACK GAS VOLUME (DRY), ACT. CFM. 49292.5
STACK GAS VOLUME 9 29.92 IN. M6 AND 68 06. F
(DRY) 26585.3
(MET) 30210.6
>
I
-------
SAMPLE CALCULATIONS
STMBOLSl
AREA CROSS-SECTIONAL STACK AREA, SO FT
BPRES BAROMETRIC PRESSURE* IN H6
OELP DELTA P
OIA DIAMETER OF CIRCULAR STACK* IN
DIM1 LENGTM OF RECTANGULAR STACK, IN
DIM2 MIDTH OF RECTANGULAR STACK, IN
MOIST MOISTURE CONTENT
MM MOLECULAR HEIGHT
NP NUMBER OF TRAVERSE POINTS
BH MOLE FRACTION MATER VAPOR
PTC PITOT TUBE COEFFICENT
SPRE8 STATIC PRESSURE, IN H20
STEMP STACK TEMPERATURE, DEC F
STPRES STACK PRESSURE, IN MG
8TVEL STACK VELOCITY, AFPM
TEMP TEMPERATURE, DEG F
VH VELOCITY HEAD, IN H20
SVOLFLN STANDARD VOLUMETRIC FLON (MET), ACFM
VOLFLM VOLUMETRIC FLON (MET)* ACFM
SVOLFLO STANDARD VOLUMETRIC FLOM (DRY)* OSCFM
FORMULAS AND SAMPLE CALCULATIONS!
SUM (SORT(VH • TEMP)) 88.8
Ofil» « —————— m .......... • T.4
NP 12
STPRES- » BPRES + (SPRES/13.6) » 29.39 * ( -1.20/13.6) • 29.3 IN HG
SUM (STEMP) 5985.
STEMP « —..——.— * ——— • «99. DEG F
NP 12
3.141ft * (DIA/2)**2 3.1416 * ( 97.300/2)**2
AREA(CIRCULAR STACK) • ———————— • ————— « 91.849 SQ FT
_ 144 140
85.49 * PTC * OELP 85.49 * .83 • 7.4
STVEL « ———— c .........—...—— • is.Q AFPM
SORT (MM * STPRES) SORTt 29.00 * 29.3 )
VOLFLM * 60. • STVEL * AREA • 60. * 18.0 • 51.849 « 56014.3 ACFM
SVOLFLM « VOLFLM * STPRES • ( 460. * 68. ) 56014.3 * 29*3 * ( 460. * 68. )
................................ • .................................. • 30210.6 ACFM
29.92 • ( STEMP » 460. ) 29.92 • ( 498.8 * 460. )
SVOLFLO • SVOLFLM * (1. - 8M) • 30210.6 • (1 - .12) * 26585.3 OSCFM
-------
FIELD OAT*
I
M
u>
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO. 1 COKE BATTERY STACK
SAMPLE TYPE PART/H2S04/S02
OPERATOR BRUFFEY
AMBIENT TEMP. (DEG.F) 62.
BAR. PRESS. (IN. HG) 29.39
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530115
STACK INSIDE DIM. (IN) 97.50 .00
P1TOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 3 5.0 IN.HG
METER CALIB. FACTOR 1.003
READ » RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INI? "
SAMPLE
TIME
(MIN.)
0~~
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
f i n^ tf i
CLUCK!
~ 910
920
930
9ao
950
1000
1010
1020
1030
1040
1050
1100
iiio
GAS METER
READING
(CU.FT.)
6 5 6. "4 7 2
661.630
666.670
6M.720
677.260
682.630
687.920
693.050
698.130
703.250
708.370
713.970
720.086
VELOCITY
HEAD
(IN.H20)
. ..
.060
.060
.060
.070
.070
.060
.060
.060
.060
.060
.070
.090
ORIFICE
PRESSUHE
DIFFERENTIAL
(IN.
DESIKED
.76
.72
.72
.87
.87
.72
.72
.72
.72
.72
.87
1.11
H20)
ACTUAL
.76
.72
.72
.87
.87
.72
.72
.72
.72
.72
.87
1.11
STACK
TEfP
(DEG.F)
519.
538.
545.
545.
555.
550.
520.
535.
510.
544.
556.
520.
DATE 10/27/81
RUN NUMBER 1-1
PROBE LENGTH ft TYPE 5* HEATEU GLASS
NUZZLE 1 t I.D. .398
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER U
KtTER BOX NUMBER FU2
KttEH Ht»0 OIFF. 1.76
C FACTOR .86
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .15
OHY GAS MEIER
TEMP
(DEG.F)
ULEI OUTLET
67. 67.
66. 68.
72. 68.
75. 68.
76. 7U.
77. 71.
78. 72.
78. 72.
78. 7cf.
79. 73.
79. 73.
79. 73.
PUMP
VACUUM
(IN.HG)
2.0
2.U
3.0
3.0
2.0
3.0
3.5
3.6
3.6
3.6
3.6
3.6
SAMPLE
BOX TEMP
(OEG.F)
270.
256.
212.
256.
255.
248.
249.
251.
252.
250.
244.
250.
IMPINGEK
TEMP
(DEG.F)
54.
55.
53.
52.
54.
54.
55.
52.
53.
52.
53.
52.
TOTALS
AVERAGE
120.0
63.614
.79
.79 537.
76.
71,
3.0 252.
53.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
1-1
NO. 1 COKE BATTERY STACK
TEST DATE
TB
TF
TT
NP
V
ON
___CP
PM
> VM
1
TM
VMSTD
VLC
VHC
BNO
FMD
PC02
P02
PCO
PN2
MD
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
~ PERCENT MOISTURE BV VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 Bv VOL., DRV
PERCENT CO BV VOL., DRV
PERCENT N2 BV VOL., DRY
MOLECULAR MT-ORY STACK GAS
MOLECULAR KT-3TACK GAS
ENGLISH UNITS
10/27/81
1110
120.0
12
1.003
.398 IN
.84
.79 IN-H20
63.614 CU-FT
73.0 F
62.205 SCF
fST.S
8.731 SCF
12.31
.677
4.20
1C. 50
.00
85.30
29.0«
27.73
METRIC UNITS
10/27/81
910
1110
120.0
12
1.003
10.1
.84
20.2
1.601
22.6
1.761
185.5
.247
12.31
.877
4.20
10.50
.00
85.30
29.09
27.73
CM
CM-H20
CU-M
C
SCI"
sec
-------
PB BAROMETRIC PRESSURE
PSI 'STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS "~" AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLOW RATE* DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 DEC F, 29.92 IN.HG.
29.39 IN-HG
•1.20 IN-H20
29.30 IN-HG
537. F
20.2 FPS
7466. SQ-IN
171B626. SCFH
3777201. ACFH
108.b
.0
.0000 GR/OSCF*
.000 LB/HR
716.51 KM-HG
-30.as cf-nao
7aa,26 CK-HG
280. c
6.2 fPS
a.817 SO-M
08666. SCMH
106960. »CHH
108.6
.0
.000 CG/OSO
.00 KG/HK
I
M
Ul
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 1-1
NO. 1 COKE BATTERY STACK
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VMSTD '• (17.647 • VM * Y * IPB * PM / 1S.6J) / (TM •» 460.)
17.607 * 63.614 * 1.003 * ( 24.39 » .793 / 13.6)
VMSTD » —————— — ......_.— ....................... - t>^.^o'3 uscf
( 73. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC • .04707 * VLC
VHC i .04707 * i86. * 8.73 SCF
PERCENT MOISTURE IN STACK GAS
BHO «~ (100. * VHC) / (VMStb * VHC)
100. * 6. 73
I BNO * - ------- — • ---- — ------- s 12.31 PERCENT
62.205 * 8.73
(Ti
MOLE FRACTION OF DRY STACK GAS
FMD e (100. - BMO) / 100.
100. - 12.3
FMD * -— --- — — — --- — s .877
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO « (PC02 * .44) » (P02 * .32) * (PN2 * PCO) * .28
MD * ( 4.20*44/100) » (10.5*32/100) * ((85.3+ .0) * 28/100 = 29. 09
MOLECULAR HEIGHT OF STACK GAS
MHS 8 MD * (1. • (BHO/100)) * 18. * (BNO/100)
MWS * 29.09* (1. -(12.31/100)) «• 10. * (12.31/100) a 27.73
-------
STACK 6*3 VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SORTtVH * ITS * 160.))
VS s 85.49 * CP • DELP / ISQRT(MMS * PS) • PNTS)
VS * 85.49 * .84 * 96.387 / (SORH 27.73 * 29.30) * 12. = 20.21 FPS
STACK GAS VOLUMETRIC FLOM AT STACK CONDITIONS
OS = VS * AS • 3600/144
OS * ~ 30.24 • 7466. 3600/144 * 3777241. ACFH
STACK CAS VOLUMETRIC FLOM AT STANDARD CONDITIONS
OSSTtT* if.647 • OS • PSr
-------
Run No. 1.1
Sample volume = 1.76 m3. 62.21 scf
Example calculations
CS (Part) =227.1/1.76 = 129.0 rna/m3
CS (Part) = 0.001 x 227.1x 15.43/62.21 = 0.56 qr/dscf
CS (S02) =1960 /I.76 =1113,6mQ/m3
=1113.6x 24.06/64 = 419ppm
= 0.001 x 1960x 15.43/£2L^L_ = 0.486 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
226.9
81.5
111.4
1960
8.9
3 Concentration,
mg/m
128.9
46.3
63.3
1113.6
5.0
gr/dscf
0.056
0.020
0.028
0.486
0.002
ppm
419
1
A-18
-------
FIELD DATA
vo
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l CUKE BATTERY STACK
SAMPLE TYPE PART/M2S04/SU2
OPERATOR BRUFFEY
AMBIENT fEMP. (DEC. F) 62.
BAR. PRESS. UN. H6) 29.39
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530019
STACK INSIDE DIM. (IN) 97. 50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .001 CFH 9 6.0 IN.HG
METER CALIB. FACTOR I. 091
READ » RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE STACK
POINT TIME TIME READING HEAD DIFFERENTIAL TEMP
NO. (MIN.) (24-HR (CU.FT.) (IN.H20) (IN.H20) (DEG.F)
INlf ~ 0""
10.0
20.0
30.0
40.0
50.0
60.0
70.0
ao.o
90.0
100.0
110.0
120.0
1*1. Vl*n /
91a —
924
934
944
954
1004
~ 1014
1024
1034
1044
1054
1104
1114
DESIRED
902.817
907.590
912.260
917.320
922. 400
927.530
932.230
936.910
941.610
946.760
951.470
956.660
961.326
._ — ...
.060
.060
.070
.070
.070
".060
.060
.060
.070
.060
.070
.060
.._ .
.76
.72
.87
.87
.87
.72
.72
.72
.87
.72
.87
.72
ACTUAL
.76
.72
.87
.87
.87
.72
.72
.72
.87
.72
.87
.72
DATE 10/27/01
HUN NUMBER 1-2
PHOBE LENGTH ft TYPE 5' HEATED GLASS
NUZZLE 2 : I.D. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBEH 0
PETER BOX NUMBER FBI
METER MEAD DIFF. i.ao
C FACTOH .86
PROBE HEATER SETTING 250.
HEAIER BOX SETTING 250.
REFERENCE PRESS. DIFF. .15
DHY GAS METER PUMP SAMPLE IMPINGEH
TEMP VACUUM BOX TEMP TEMP
(DEG.F) (IN.HG) (OEG.F) (DEG.F)
INLET OUTLET
527.
541.
542.
549.
561.
515.
523.
538.
533.
550.
562.
520.
72.
71.
76.
80.
81.
83.
83.
84.
84.
8«.
84.
83.
-
73.
73.
74.
75.
75.
76.
76.
77.
78.
78.
79.
78.
.5
.5
.5
.0
.0
.0
.0
.0
.0
.0
4.0
4.0
*
283.
245.
263.
253.
255.
260.
251.
255.
253.
258.
258.
254.
49.
50.
49.
50.
51.
52.
54.
53.
52.
51.
50.
50.
TOTALS
AVERAGE
120.0
58.511
.79
.79 538,
80.
76.
3.9 257.
51.
-------
PARTICULATE FIELD DATA & RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BHUFFEY
TEST
1-2
NO.I COKE BATTERY STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
>
1
M VM
O
TM
VM3TD
VLC
VMC
BMO
FMD
PC02
P02
PCO
PN2
MD
MHS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GELjML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT ~MOI3tUR£ BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL.* DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR WT-STACK GAS
ENGLISH UNITS
10/27/81
914
1114
120.0
12
1.044
.397 IN
•ea
.79 IN-H20
58.511 CU-FT
78.2 F
58.981 SCF
iS5~.7
8.741 SCF
12.91
.871
4.20
10.50
.00
85.30
29.09
27.66
METRIC UNITS
10/27/81
914
Ilia
120.0
12
1.044
10.1
.84
20.0
1.657
25.7
1.670
185. 1
.248
12.91
.871
4.20
10.50
.00
85.30
29.09
27.66
KM
MM-H20
CU-M
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
P3I STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLOH RATEt DRY*
OS ACTUAL STACK FLOH RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 66 DEC F, 29.92 IN.HG.
29.39 IN-HG
M.20 IN-H20
29.30 IN-HG
538. F
FP3
SO-1N
SCFH
ACFH
20.2
7466.
1698840.
3766316.
104.7
.0
.0000 GR/D3CF*
.000 LB/HR
746.51 MM-HG
-30.48 KM-H80
744.26 CM-HG
281. C
6.2 PPS
4.817 30-M
48106. SOH
106651. AC»>H
104.7
.0
.000 PG/DSCP
.00 KG/HH
I
NJ
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 1-2
NO.l COKE BATTERY STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO « (17.647 • VM * Y * (PB * PM / 13.6)) / (TM » 460.)
17.647 • 50.511 * 1.044 • ( 29.39 * .766 / 13.6)
VMSTO » ——————— — — — — ——— — — — — — -. = 58.981 OSCF
( 78. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VtlC * .04707 * VLC
VHC V .04707 • 186. » 8.74 3CF
PERCENT MOISTURE IN STACK GAS
BHO"* (100. • VMC) / (VMSTD * VWC)
100. • 0.74
> BKO » — • — — » 12.91 PERCENT
I SB.981 * 8.74
N3
to .... ... ..
MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BHO) / 100.
100. - 13.9
FMD « ————— » .871
100.
AVERAGE M6LECULAW~N'ClftHT~3F" DRV STACK
MD a (PC02 * .44) * (P02 * .32) » (PN2 * PCO) * .28
MD * ( 4.20*44/100) « (10.5*32/100) * ((85.3* .0) * 28/100 z 29.09
MOLECULAR HEIGHT OF STACK GAS
MhS > MD * (1. • (BHO/100)) * 18. * (BWO/100)
MMS * 29.09* (1. -(12.91/100)) * 18. » (12.91/100) s 27.66
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP * SUM. OF THE SQRTCVH * (TS * 460.))
VS » 83.49 * CP * OELP / (SORT(MWS • PS) • PNTS)
VS * 85.49 * .84 * 95.993 / (SORT( 27.66 * 39.30) * 12. = 20.18 FPS
STACK 6AS VOLUMETRIC FLOM AT STACK CONDITIONS
OS s VS • AS • 3600/144
OS « 20.18 * 7466. 3600/144 • 3766316. ACFH
STACK GAS VOLUMETRIC FLOM AT STANDARD CONDITIONS
OSSTD « 17.647 «i d$ * PS 5 (1. - (BHO/KTOj) / (TS * 460.)
17.647 * 3766316. * 29.30 * (1. • (12.91/100))
OSSTD « .-...—.-..-..—..-...—. — — .-.-—.— ...... = 1698640. SCFH
( 538. * 460.)
PERCENT ISOKINETIC
>
I ISO a (305.SB«(TS*460.))«((0.002669»VLC)*(V**Y*(PB*(PM/13.6))/(TM*«I60.)))/(TT«VS*PS«DN«DN)
N>
W (30S.58«( 538.«460.))*((0.ti02669i~~186.)+( 58.511*1.044«C 29.39»( .786/13.6))/( 78.«460.)))
ISO » — • — ——— ............. . . . ... . * 104.71 PERCENT
120. * 20.18 • 29.30 • .397 * .397
PARftCULATE LOADtNfi ••'EPA METHOD 5 (AT STANDARD CONDITIONS)
CS » 0.001 * MN * 15.43 / VMSTD
CS * 0.001 * .0 * 15.43 / 58.981 c .000 GR/OSCF
PARTICULATE LBS/HR •• EPA METHOD 5
PMR * CS • OSSTD / (15.43 • 453.6)
PMR s .000 * 1698840. / (15.43 • 153.6) « .00
-------
3
Run No. 1.2
Sample volume = 1.67 m r 58.98 scf
Example calculations
CS (Part) =192.8 / 1.67= 115.4 m/m-
CS (Part) = 0.001 x 192.8X 15.43/58.98 = 0.050 qr/dscf
CS (S02) =1850 / 1.67=n07.8mq/m3
=1107.8X 24.06/64 = 416DDm
= 0.001 x1850 x 15.43/58.98 = 0.484 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
192.8
55.2
7.4
10.1
1850
9.4
, Concentration,
mg/m
115.4
33.0
4.4
6.1
1107.8
5.6
gr/dscf
0.050
0.014
0.002
0.003
0.484
0.002
ppm
416
1
A-24
-------
FIELD DATA
I
NJ
tn
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TTPE I-3-M8-350
OPERATOR CLARKE
AMBIENT TEMP.(OEG.F) 72.
BAR. PRESS. (IN. HG) 29.39
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530092
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .61
THERM. NO.
LEAKAGE .000 CFM 8 3.5 IN.HG
METER CALI8. FACTOR .992
READ » RECORD DATA EVERT 10.0
TRAVERSE
POINT
NO.
INIT
OTALS
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
ao.o
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
120.0
CLOCK
TIME
(20-HR
r i nrv 1
ULUIR J
910 ~
920
930
940
950
1000
1010
1020
1030
1040
1050
1100
1110
GAS METER
READING
(CU.FT.)
410.667
416.000
421.475
425.775
430.695
435.595
440.777
445.910
450.024
455.667
460.660
466.500
471.932
61.065
MINUTES
VELOCITY
HEAD
(IN.H20)
.060
.060
.060
.070
.070
'.060
.060
.060
.060
.060
.070
.090
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.78
.78
.78
.87
.87
.78
.78
.78
.78
.78
.87
i.io
H2U)
ACTUAL
.76
.78
.78
.87
.87
.76
.78
.78
.78
.78
.87
1.10
STACK
TEfP
(DEG.F)
519.
536.
545.
545.
555.
550.
520.
535.
510.
544.
558.
516.
DATE 10/27/81
HUN NUMBER 1-3
PKOBE LENGTH « TYPE 5FT GLASS HEAltO
NUZZLE 3 > l.D. .394
ASSUMED MU1S1UHE 12.0
SAMPLE BUX NUMBER
PETER BOX NUMBER FBI
*ETEH MEAD D1FF. 1.87
C FACTOH .88
PROBE HEATER SETTING 35U.
HEATER BOX SETTING 350.
REFEHENCE PRESS. DIFF. .15
OHY GAS METER
TEMP
(DEG.F)
ULET OUTLET
68. 63.
70. 63.
73. 64.
76. 61.
78. 66.
80. 66.
80. 66.
80. 67.
80. 68.
80. 66.
80. 68.
78. 60.
PUMP
VACUUM
(IN.HG)
2.0
2.0
2.0
2.0
2.0
2.0
2.V
2.0
2.0
2.0
3.0
3.5
SAMPLE
BOX TEMP
(DEG.F)
306.
337.
3«6.
3«7.
344.
341.
337.
345.
3«5.
336.
337.
335.
IMPINGEH
TEMH
(DEG.F)
52.
40.
40.
40.
42.
42.
42.
44.
4b.
46.
46.
4«.
AVERAGE
.83
.83 536.
77.
65.
2.2
338.
44.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
1-3
COKE OVEN OUTLET
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1 VM
(Ti
TM
VMSTD
VLC
VWC
BHO
FMO
PC02
P02
PCO
PN2
MD
MHS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
fdtAL H2o couecTE6 IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL.* DRY
PERCENT 02 8Y VOL.i DRY
PERCENT CO BY VOL.* DRY
PERCENT N2 BY VOL., DRY
MOLECULAR MT-OftV STACK GAS
MOLECULAR MT-STACK GAS
10/27/81
910
1110
120
12
61
71
59
m
10
15
4
10
85
29
27
.0
.99Z
.394 IN
.84
.83 IN-H20
.065 CU-FT
.1 F
.280 SCF
i3
.981 SCF
.63
.844
.20
.50
.00
.30
.09
.36
METRIC UNITS
10/27/81
910
1110
120
12
10
21
1
21
1
233
15
4
10
85
29
27
.0
.992
.0
.84
.1
.729
.7
.679
.3
.311
.63
.844
.20
.50
.00
.30
.09
.36
KM
(HM-H20
CU-M
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
P8I STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLOW RATE* DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT I30KINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 DEC F, 29.~9ir~iN~.~Hl;.
29.39 1N-HG
-1.20 IN-H20
29.30 IN-HG
536. F
20.0 FPS
7066. SQ-IN
1665014. SCFH
3801518. ACFH
109.0
.0
.0000 GR/DSCF*
.000 LB/HH
706.51 *M-HG
-30.48 *
740.26 MM-HG
260. C
6.2 WPS
0.817 30-M
07106. SCMH
107648. »OH
109.0
.0
.000 PG/DSCP
.00 KG/HM
I
NJ
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 1-3
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD » (17.647 * VM * Y • (PB * PM / 13.6)) / (TM * 460.)
17.647 * 61.065 * .992 * ( 39.39 «• .829 / 13.6)
VMSTO « —————— — . — — - — — — — . — — — — -.-...-. s 59.380 OSCF
I ' 71. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC » .04707 * VLC
VWC « .04707 * 235. « ~Td.98 SCF
PERCENT MOISTURE IN STACK GAS
BWO « (100. * VNC) / (VMSTD # VHC)
100. * 10.90
^ BNO * — ------- — --- — — — - = 15.63 PERCENT
I 59.3BO * 10.98
NJ
00 .......... ------ ......
MOLE FRACTION OF DRY STACK GAS
FMD s (100. - BNO) / 100.
.~i 15.6
FMD « — - ---- — --- — — — « .844
100.
AVERAGE MOLECULAR HEIGHT OF Gftv STACK GAS
MD a (PC02 * .44) * (POZ * .33) * (PN3 + PCO) * .38
MD s ( 4.ZO*44/100) * (10.5*32/100) * ((85.3* .0) * 38/100 = 39.09
MOLECULAR WEIGHT OF STACK GAS
MMS s MD * (1. - (BNO/IOO)) * 18. * (BNO/100)
MNS * 39.09* (i. -(15.63/100)) 4 18. * (15.63/100) * 27.36
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE SORTIVH * US * 460.))
V3 » 85.49 • CP • DELP / (SQRT(MWS * PS) • PNTS)
VS a 85.49 * .84 * 96.360 / (SORT( 37.36 * 39.30) * 13. = 20.37 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS ' VS * AS * 3600/144
OS * 80.37 * 7466. 3600/144 a 3801518. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
03STD « 17.647 • OS • PS • (17- IBNO/lOO)) / (TS » 460.)
17.647 * 3801518. « 29.30 • (1. - (15.63/100))
03STD • ————————— ——————— — — — = 166S01U. SCFH
( 536. * 460.)
PERCENT ISOKINETIC
> ISO « (305.58*(TS+460.))»((0.002669*VLC)'»(VM*Y*(PB*(PM/13.6))/(TM*
-------
Run No. 1.3
Sample volume = 1.68m3f 59.28 scf
Example calculations
CS (Part) = 72.9/1.68 = 43.4 mq/m3
CS (Part) = 0.001 x_73 x 15.43/59.28 = 0.019 qr/dscf
CS (S02) = 1870 / 1.68 = 1113.bo/m3
=1113.1 x 24.06/_64_ = 418 ppm
= 0.001 x1870 x 15.43^9.28 = 0.487gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
72.9
9.8
13.4
1870
65.4
3 Concentration,
mg/m
43.4
5.8
8.0
1113.1
38.9
gr/dscf
0.019
0.002
0.003
0.487
0.017
ppm
4.18
10
A-30
-------
FIELD DATA
I
u>
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 1-4-M8-350
OPERATOR CLARKE
AMBIENT TEMP. (DEG.F) 72.
BAR. PRESS. (IN.HG) 29.39
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530072
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 5.0 IN.HG
METER CALIB. FACTOR 1.010
READ I RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT TIME
NO. (MIN.)
INlf 0"
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
TIME"
(20-HR
- §U-
924
934
944
954
1004
ioi4 —
1024
1034
1044
1054
1104
1114"
READING
(CU.FT.)
838.960
843.665
848.801
853.800
858.673
863.750
868.473
873.392
878.250
883.476
888.380
893.725
898.155
HEAD
(IN.H20)
.060
.060
.070
.070
.070
.060
.060
.060
.070
.060
.070
.060
DIFFERENTIAL
(IN.
DESIRED
.78
.78
.87
.87
.87
.r*
.78
.78
.87
.78
.87
.78
H20)
ACTUAL
.78
.78
.87
.87
.87
.78
.78
.78
.87
.78
.87
.T8
STACK
TEMP
(DEG.F)
527.
541.
532.
509.
561.
516.
523.
538.
533.
550.
562.
521.
DATE 10/27/81
KUN NUMBER i-o
PROBE LENGTH » TYPt 6FT GLASS HEATED
NOZZLE 0 < 1.0. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBEH
METEN BOX NUMBtR FB5
METEN HEAD DIFF. 1.86
C FACTOR .88
PROBE HEATER SETTING 350.
HEATER BOX SETTING 35u.
REFERENCE PRESS. DIFF. .15
OHY GAS METER PUMP SAMPLE IMPINGEH
TEMP VACUUM
(DEG
INLET
71.
71.
70.
76.
80.
81.
82.
82.
82.
83.
82.
80.
.F) (IN.HG)
OUTLET
72. 1.0
71.
72.
72.
72.
73.
70.
75.
7b.
77.
76.
75.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(OEG.F)
277.
338.
339.
342.
348.
344.
342.
345.
339.
339.
332.
341.
TEMP
(DEG.F)
52.
52.
50.
50.
56.
50.
50.
56.
56.
5B.
58.
60.
TOTALS
AVERAGE
120.0
59.195
.82
.82
538.
79.
74.
1.0
336.
55,
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT» NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
1-4
COKE OVEN OUTLET
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
> VM
OJ
TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
ENGLISH UNITS
10/27/81
914
1114
120.0
12
1.010
.397 IN
•««
.82 IN-H20
59.195 CU-FT
76.2 F
37.947 SCF
METRIC UNITS
10/27/81
914
Ilia
120.0
12
1.010
10.1
.84
20.8
1.676
24.6
1.641
VM
VM-H20
CU-M
C
SCM
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VMC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY " VffLVi DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRV
MD MOLECULAR XT-DRY STACK GAS
MMS MOLECULAR HT-STACK GAS
165.0
7.767 SCF
165.0
.22U SCP
11.82
.882
4.20
10.50
.00
as. 30
29.09
27.78
11.82
.882
4.20
10.50
.00
85.30
29.09
27.78
-------
PB
PSI
PS
T8
VS
AS
OSSTD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOM RATE, DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKIMETIC
FILTERABLE PART
MG. EPA 5
FILTERABLE PART
FILTERABLE PART
29
.....
29
538
"26
7466
1716865
3756751
101
.39
.20
.30
•
.1
IN-HG
IN-H20
IN-HG
f
FPS
SO-IN
•
•
.8
.0
.0000
.000
SCFH
ACFH
GR/OSCF*
L8/HR
746
-30
744
281
6
4
48616
106381
101
.51
.48
.26
•
.1
.817
•
•
.8
.0
.000
.00
MM-HG
*M-H20
PM-HG
C
SQ-M
SCUM
• C*H
^G/USC*
KG/HH
EMISSION RATE
• 68 DIG Fr 29.92 IN.H6.
U)
OJ
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 1-1
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 * VM * Y • (P8 * PM / 13. fc)) / ITM * 460.)
17.647 • 59.195 * 1.010 * ( 39.39 * .818 / 13.6)
VMSTO « ————— ———— — ............. ---- ........ - 57.«» 57.947 * 7.77
I
U) • - ------ - ......... — -
*>
MOLE FRACTION OF DRY STACK GAS
FHD * (100. - BMO) / 100.
loo. • ii.e
—— • .882
100.
AVERAGE MOLECULAR NEt§Hf OF DRY STACK GAS
MD s (PCOa * .44) «• (P02 * .32) * (PN2 » PCO) * .28
MD z ( 4.20*44/100) * (10. 5*32/100) » ((65.3* .0) * 28/100 = 29.09
MOLECULAR WEIGHT OF STACK GAS
MMS • MD * (1. • (BMO/100)) » 18. * (BMO/100)
MWS s 29.09* (i. -(11.82/100)) » 18. * (11.82/100) * 27.78
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SORTIVH • (TS * 460.))
VS = 8S.49 * CP * OELP / (30RT(MKS • PS) * PNTS)
VS = 85.49 * .84 * 95.959 / CSOHTC 37.78 • 29.30) * 12. = £0.13 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS * 20.13 * t466. 3600/144 • 3756791. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTD « 17.64? * 0$ • ?3 • (1. - (BMO/100)) / (TS + 460.)
17.647 • 3756791. * 29.30 * (1. - (11.62/100))
OSSTD » —..————............. —........... ... . - 1716665. SCFH
( 538. » 460.)
PERCENT ISOKINETIC
> ISO * (305.58*(TS*460.))*((0.002669*VLC)*(VM*Y*(PB»(PM/13.6))/(TM*460.)))/(TT*V9*P8*DN*DN)
I
J£ (305.58*( 538.*460.))*((0.0026698" 165.)»( 54.195*1.010*( 29.39+( .818/13.6))/( 76.«460.)))
ISO • ——————————--—•——— — --- — ------——---------—- — --- — — -------- — - — s 101.80 PERCENT
120. * 20.13 • 29.30 * .397 • .397
PARTICULAR LOADING -- EPA METHOD 5 (AT STANDARD CONDITIONS)
CS e 0.001 • MN • 15.43 / VMSTO
CS * 0.001 * .0 * 15.43 / 57.947 • .000 GR/DSCF
PARTICULATE LBS/HR •• EPA METHOD 5
PMR * CS * OSSTD / (15.43 • 053.6)
PMR « .000 • 1716865. / (15.43 * 453.6) « .00
-------
Run No.1.4
Sample volume =1.64 nT% 57.95 scf
Example calculations
CS (Part) = 50.6/1.64 = 30.8 mq/m3
CS (Part) = 0.001 x50.7 x 15.43/57.95 = 0.013 qr/dscf
CS (S02) = 1810/1.64 =1103.7ma/m3
=1103.7X 24.06/64 =415 ppm
= 0.001 x 1810 x 15.43/57.95 = 0.482 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
50.6
4.7
6.4
1810
56.0
2 Concentration,
mg/m
30.8
2.9
3.9
1103.7
34.1
gr/dscf
0.013
0.001
0.002
0.482
0.015
ppm
415
8
A-36
-------
FIELD DATA
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE OVEN STACK
SAMPLE TYPE METHOD 5-250
OPERATOR 00
AMBIENT TEMP. (DEC. F) 62.
BAR. PRESS. (IN.HG) 29.39
STATIC PRESS. (IN. H20) .00
FILTER NUMBER(S) 3530066
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .64
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
READ • RECORD DATA
TRAVERSE SAMPLE
POINT TIME
NO. (MIN.)
INIT 0 ~
10.0
20.0
30.0
40.0
50.0
60.0
70.0
70.4
CLOCK
TIME
(24-HR
PI t\f tf i
CLUCK)
947
957
1007
1017
1027
1037
1047
1057
1057
.000
1.033
EVERT 10.0
GAS METER
READING
(CU.FT.)
593.361
600.570
607.750
614.950
622.140
629.310
636.500
643.640
644.151
CFM 8 6.
MINUTES
VELOCITY
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.050
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.81
.81
.81
.81
.81
.81
.81
1.81
H20)
ACTUAL
.81
.81
.81
.81
.81
.81
.81
.81
STACK
TEMP
(OEG.F)
550.
550.
550.
550.
550.
550.
550.
550.
DATE 10/27/81
HUN NUMBER 1-5
PROBE LENGTH A TYPE 6* GLASS
NOZZLE 6-103S I.D. .520
ASSUMED MOISTUHE 11.0
SAMPLE BOX NUMBER
KETEH BOX NUMBER FB4
METEH HEAD OIFF. 1.68
C FACTOR .92
PRUBE HEATER SETTING 250.
HEATER eux
REFERENCE
DRY GAS METER
TEMP
(DEG.F)
INLtT OUTLET
-•
77. 77.
74. 75.
76. 74.
78. 73.
80. 74.
80. 74.
80. 74.
80. 74.
SETTING
250.
PRESS. DIFF. .05
PUMP
VACUUM
(IN.HG)
4.7
5.1
5.2
5.3
5.3
5.3
5.5
5.5
SAMPLE
BOX TEMP
(DEG.F)
230.
288.
29U.
291.
262.
240.
253.
253.
IMPINGEH
TEMP
(DEG.F)
38.
40.
«0.
50.
50.
54.
52.
52.
TOTALS
AVERAGE
70.4
50.790
1.61
1.81
550.
78.
74,
5.2
263,
47,
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO
TEST
1-5
COKE OVEN STACK
TEST DATE
>
1
U)
00
TB
TF
TT
NP
V
ON
CP
PM
VM
TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
ENGLISH UNITS
10/27/61
947
1057
70
8
1
1
SO
76
50
.4
.033
.520 IN
.84
.81 IN-H20
.790 CU-FT
.3 F
.973 SCF
METRIC UNITS
10/27/81
947
1057
70.
8
1.
13.
•
4b.
1.
24.
1.
4
033
2
84
0
438
6
443
KM
MM-H20
CU-M
C
SCM
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GELrML,
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BV VOCUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BV VOL.r DRV
P02 PERCENT 02 BY"VOL., DRY
PCO PERCENT CO BV VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR MT-ORY STACK GAS
MHS MOLECULAR MT-STACK GAS
169.5
7.978 SCF
169.5
.226 Sen
13.53
.865
4.20
10.50
.00
85.30
29.09
27.59
13.53
.865
4.20
10.50
.00
85.30
29.09
27.59
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD . STACK FLOW RATE* DRY*
OS ACTUAL STACK FLO* RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 3
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68~DCG F, ~Z~
29.39 IN-HG
.00 IN-H20
Z9.39 IN-HG
550. F
17.9 FPS
7066. SO-IN
1485328. 3CFH
3345007. ACFH
102.8
.0
.0000 GR/DSCF*
.000 LB/HR
746.51 *M-HG
.00 PM-H20
746.51 PM-HG
288. C
5.5 KPS
4.817 SO-M
12057. SON
94721. *CKH
102.8
.0
.000
.00 KG/MR
I
OJ
VD
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 1-5
COKE OVEN STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO « (17.647 • VM * Y * (PB » PM / 13.6)) / (TM * 460.)
17.647 • 50.790 * 1.033 * ( 39.39 * 1.810 / 13.6)
VMSTD * ————— — • — • a 50.973 DSCF
( 76. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC « .04707 * VLC
VNC « .04707 * 170. « "~7.98 SCF
PERCENT MOISTURE IN STACK GAS
BHO » (100. * VMCJ / (VMStD * VHCT
100. * 7.98
BHO « ————— ......... s 13.53 PERCENT
50.973 * 7.98
MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BNO) / 100.
loo. - rs.s
FMD * —————......... • .865
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK CAS
MD « (PC02 * .44) * (POZ * .33) * (PNZ • PCO) • .28
MD * ( 4.20*44/100) * (10.5*32/100) » ((85.3* .0) * 28/100 = 29.09
MOLECULAR HEIGHT OF STACK GAS
MNS a MD * (1. - (BNO/100)) » 18. • (BNO/100)
MH3 * 29.09* (1. •(13.53/100)) * 18. * (13.53/100) « 27.59
-------
STACK G»3 VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE 30RTIVH * ITS » 460.))
VS * BS.49 • CP * OELP / (SQRT(MHS • PS) * PNTS)
VS 3 65.49 * .84 • 56.651 / (SQRM 27.59 * 29.39) * 8. = 17.92 FPS
STACK GAS VOLUMETRIC FLOH AT STACK CONDITIONS
QS * VS • AS * 3600/144
OS 3 17.92 * 7466. 3600/144 x 3345001. ACFH
STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO » 17.647 • 03 •P8"^(T7i (BNO/100)) / (TS * 460.)
17.647 • 3345007. • 29.39 • (1. - (13.53/100))
03STD » ———————————————— — — — a 1485226. SCFH
( 550. * 460.)
PERCENT ISOKINETIC
ISO « (30S.5B«(TS*460.))*((0.002669«VLC)«(VM<»Y*(PBMPM/13.6))/(TM+460.)))/(TT«VS*P3*DN*Df»)
(305.58M: 5$6.*460.))M(0.602669« 170.)*( 50.790*1.033*( 29.39«( 1.810/13.6))/( 7b.*060.)))
ISO * ——————................................................_.._....._......_.................. i 102.84 PkHCEMT
70. * 17.92 * 29.39 • .520 * .520
PARTICIPATE LOADING -• EPA METHOD 5 (AT ^TANDARO CONOltlONS)
CS e 0.001 * MN • 15.43 / VMSTD
CS * 0.001 • .0 • 15.43 / 50.973 = .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR * CS * OSSTD / (15.43 * 453.6)
PMR • .000 * ~I485228. / (15.43 • 453.6) » .00
-------
Run No. 1.5
Sample volume = 1.44 tn3t 50.97 scf
Example calculations
CS (Part) =135.3/1.44 = 94.0 mq/m3
CS (Part) = 0.001 x135.3x 15.43/50.97= 0.041 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ . = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
135.3
47.5
41.7
37.3
34.5
30.5
0.0
0.0
28.2
2.6
23.4
3 Concentration,
mg/m
94.0
33.0
29.0
25.9
24.0
21.2
0.0
0.0
19.6
1.8
16.2
gr/dscf
0.041
0.014
0.013
0.011
0.010
0.009
0.0
0.0
0.008
0.001
0.007
ppm
A-42
-------
FIELD OAT*
I
£>.
U)
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE UVEN STACK
SAMPLE TYPE METHOD 8-600
OPERATOR DO
AMBIENT TEMP. (DEC. F) 62.
BAR. PRESS. (IN.HG) 29.39
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530210
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 8 21.
METER CALIB. FACTOR .982
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT
NO.
INIT
TIME
(MIN.)
6
10.0
20.0
30.0
40.0
50.0
60.0
64.5
TIME
(24-HR
f i nf M \
LLUCKJ
958"
1008
1018
1028
1038
1048
1058
1102
READING
(CU.FT.)
88.938
98.960
107.100
115.080
122.680
130.090
137.250
140.342
HEAD
(IN.H20)
._. .._ ..
.050
.050
.050
.050
.050
.050
.050
CLEVELAND
0 IN.HG
ORIFICE PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.66
.66
.66
.66
.66
.66
.66
H20)
ACTUAL
-
3.66
2.20
2.20
2.00
1.87
1.80
1.60
STACK
TEMP
(OEG.F)
550.
550.
550.
550.
550.
550.
550.
DATE 10/27/81
NUN NUMBER t-6
PROBE LENGTH S TYPE 4* QUARTZ
NUZZLE t I.U. .620
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBER FB8
METER HEAD DIM . 1.91
c FACTOR .94
PROBE HEATER SETTING 600.
HEATER BOX SETTING 600.
REFERENCE PRESS. DIFF. .02
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP
(DEG
IM.E!
64.
68.
70.
71.
71.
71.
70.'
.F)
OUTLET
63.
63.
63.
64.
65.
65.
65.
VACUUM
(IN.HG)
9.6
13.9
17.7
19.4
19.7
19.8
20.2
BOX TEMP
(DEG.F)
624.
653.
612.
667.
639.
528.
535.
TEMP
(DEG.F)
38.
40.
40.
50.
50.
54.
52.
TOTALS
AVERAGE
64.5
51.404
3.66
2.19 550.
69.
64.
17.2 608.
46.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND 00
TEST
1-6
COKE OVEN STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM .
> VM
"^ TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
ENGLISH UNITS
10/27/81
958
1102
64.5
7
.982
.620 IN
_.••«
2.19 IN-H20
51.404 CU-FT
66.6 F
49.985 SCF
METRIC UNITS
10/27/81
958
1102
64.5
7
.982
15.7
.84
55.6
1.456
19.2
1.415
MM
KM-H20
CU-M
C
SCM
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VMC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOl... DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR MT-DRt STACK GAS
MMS MOLECULAR XT-STACK GAS
1 779
.843 SCF
17.9
.024 SCW
"1.66
.983
4.20
10.50
.00
85.30
29.04
28.91
1.66
.983
4.20
10.50
.00
85.30
29.09
28.91
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES* ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE* DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 29.92 iN.HG.
29.39 IN-HG
-1.20 IN-H20
29.30 IN-HG
550. F
17.5 FPS
7466. SQ-IN
1647806. SCFH
3272822.
69.8
.0
ACFH
.0000 GR/OSCF*
.000 LB/HR
746.51 PP-HG
•30.48 PK-H20
744.26 CM-HG
288. C
5.5 CPS
4.817 SO-M
46661. SOH
92677. *CHH
69.8
.0
.000
.00 KG/Hrt
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 1-6
COKE OVEN STACK
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (IT.647 • VM • Y • (PB «• PM / 13.6)) / (TM * 460.)
17.647 * 51.404 • .982 « ( 29.39 » 3.190 / 13.6)
VMSTO « .———.————.—— ——— — —— ...... x 49.9A5 D3CF
( 67. + 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC * .04707 • VLC
VHC a .04707 * 18. a.B4~SCF
PERCENT MOISTURE IN STACK GAS
BHO « (100. • VMC) / (VMStb * VHC)
100. * .84
> BMO a ——————— a 1.66 PERCENT
I 49.985 * .84
»^
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SORTIVH • (TS » 460.))
VS s 85.49 • CP • DELP / (3QRT(MH3 • PS) • PNTS)
VS * BS.49 • .84 * 49.744 / (SORT( 28.91 * 29.30) * 7. a 17.53 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS B VS * AS • 3600/144
OS * 17.53 « 7466. $600/144 • 3272622. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD » 17.647 • OS • "PS~« U. • (BNO/100)) / (TS * 460.)
17.647 • 3272822. * 29.30 •(!.-( 1.66/100))
OSSTD « ———— —————— ..... : 1*47606. SCFH
( 550. * 460.)
PERCENT ISOKINETIC
>
1 ISO • (305.58*(TS+460.))*U0.002669*VLC)+(VM*Y*(PB*(PM/13.6))/(TM«460.)))/(TT*VS*PS*DN*DN)
£*
~J * (30S.5fl«( 550.»«60.))««0.00266*«" !«.)»( 5I.404« ,982*( 29.39*( 2.190/13.6))/( 67.^460.)))
130 « .-——————————.. — — .-..—-- — — -....-...--. — .---.—.. — ...... — . s 69.78 PERCENT
65. * 17.53 * 29.30 • .620 * .620
PARTICIPATE LOADING -^EPA METHOD 5 (AT-STANDARD CONDITIONS)
C3 • O.OOt * MN • 15.43 / VMSTD
CS * 0.001 • .0 * 15.43 / 49.985 = .000 GR/OSCF
PARTICIPATE LBS/HR — EPA METHOD 5
PMR « C3 * OSSTD / (15.43 * 453.6)
PMR « .000 * 16«r806. / (15.43 • 453.6) « .00
-------
Run No. 1.6
Sample volume = 1.42 m.49.99 scf
Example calculations
CS (Part) = 27.0/ 1.42= 19.0 mq/m3
CS (Part) = 0.001 x27.0 x 15.43/49.99 « 0.008 qr/dscf
CS (S02) = 1120/1.42=788.7nig/m3
= 788.7x 24.06/54 = 296 DPm
= 0.001 x1120 x 15.43/12^2-. = 0.346 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
27.0
0.0
0.0
1120
606
3 Concentration,
mg/m
19.0
0.0
0.0
788.7
426.8
gr/dscf
0.008
0.0
0.0
0.346 ,
0.187
Ppm
296
105
Hydrogen peroxide contaminated.
A-48
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TTPE
OPERATOR
AMBIENT TEMP.(DEC.F)
BAR.PRESS.(IN.HG)
STATIC PRESS. UN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
REPUBLIC STEEL CLEVELAND
NO.l COKE BATTERY STACK
PART/H2304/S02
BRUFFEY
64.
29.30
-1.20
3530080
97.50 .00
.64
DATE
RUN NUMBER
PROBE LENGTH » TYPE
NUZZLE 2-1 t I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER
METER MEAD OIFF.
c FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
10/27/01
2-1
5* HEATED GLASS
.397
12.0
FB2
1.76
.66
250.
250.
LEAKAGE
METER CALIB. FACTOR
.001
1.003
READ » RECORD DATA EVERY 10.0
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
SO.O
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
ft nnt i
vUULK J
i|55
1405
1415
1425
1435
1445
1455 "
1505
1515
1525
1535
1545
~ 15S5
GAS METER
READING
(CU.FT.)
720.259
725.000
729.740
734.500
739.240
744.010
740.790
753.600
756.360
763.120
767.690
772.690
777.466
CFM a 5.
MINUTES
VELOCITY
HEAD
(IN.H20)
— -
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
0 IN.HG
ORIFICE
REFERENCE PRESS. DIFF. .15
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
H20)
ACTUAL
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
STACK
TEMP
(DEG.F)
525.
519.
530.
537.
535.
553.
565.
511.
522.
534.
534.
553.
DRY GAS PETER
TEMP
(OEG.F)
INLET OUTLET
67. 68.
66. 68.
70. 68.
73. 66.
74. 69.
75. 69.
75. 69.
75. 69.
75. 69.
75. 70.
75. 70.
73. 68.
PUMP
VACUUM
(IN.HG)
1.5
2.0
2.0
2.0
2.0
2.5
.0
.0
.0
.0
.0
.0
SAMPLE
BOX TEMP
(OEG.F)
250.
251.
2«9.
245.
250.
253.
249.
249.
242.
242.
237.
242.
IMPINGEH
TEMP
(OEG.F)
55.
54.
53.
53.
53.
52.
50.
51.
50.
51.
52.
50.
TOTALS
AVERAGE
120.0
57.227
.62
.62 535.
73.
69,
2.5 247.
52.
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
2-1
NO.l COKE BATTERY STACK
ENGLISH UNITS
TEST DATE 10/27/81
TB
TF
TT
NP
Y
ON
cp
PM
1 VM
cn
0
TM
VMSTD
TIME-START 1335
TIME-FINISH 1555
NET TIME OF TEST* MIN. 120.0
NET SAMPLING POINTS 12
METER CALIBRATION FACTOR 1.003
SAMPLING NOZZLE DIAMETER .397 IN
PITOT TUBE COEFFICIENT •««
AVERAGE ORIFICE PRESSURE .62 IN-H20
DROP
VOLUME OF DRV GAS SAMPLED 57.227 CU-FT
AT METER CONDITIONS
AVERAGE GAS METER TEMP 70.8 F
VOLUME OF DRY GAS SAMPLED 55.996 SCF
METRIC UNITS
10/27/81
1355
1555
120.0
12
1.003
10.1
.84
15.7
1.620
21.6
1.586
CM
CM-H2U
CU-M
C
SCf
AT STANDARD CONDITIONS*
VLC '"'TOtA'L HZ« COLLECTED IN
IMPIN6ERS AND SILICA GEL,ML,
VMC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BN6 PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRY
P02 PERCENT 62 SY~ VOL.." fcRY
PCO PERCENT CO BY VOL.* DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR NT-DRY STACK GAS
MH3 MOLECULAR NT-STACK GAS
TB9.I
8.901 SCF
189.1
.252 SCM
"13.72
.863
a. 20
"10.50
.00
85.30
29.09
27.57
13.72
.863
4.20
10.50
.00
85.30
29.09
27.57
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLOW RATE, DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5 _ _
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 OE6 F, 29.92 IN.HG.
29.90 IN-HG
•1.20 IN-H20
29.21 IN-HG
535. F
17.8 FPS
7466. SO-IN
1489327. SCFH
3331033.
113.4
.0
ACFH
.0000 GR/D3CF*
.000 LB/HR
740.22 CH-HG
-30.40 PM-H20
741.98 KH-MG
279. C
5.4 HPS
4.817 SO-M
42173. SOH
94325. ACI-H
113.4
.0
.000 KG/OSC"
.00 KG/HH
I
Ul
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 2-1
NO.l COKE BATTERY STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 * VM * Y * (PB » PM / 13.6)) / (TM » 460.)
17.647 • 57.227 * 1.003 * ( 29.30 * .620 / 13.6)
VMSTD a ..———. . ... 3 55.996 OSCF
( 71. * 460.)
VOLUME OF NATER VAPOR AT STANDARD CONDITIONS
VHC a .04707 * VLC
VHC * .04707 * 189. a 8.90 SCF
PERCENT MOISTURE IN STACK GAS
BMO a" (iOO. * VHC) / (VMSTO * VHC)
100. * B.90
IP BMO * — — —— = 13.72 PERCENT
I 55.996 «• 8.90
MOLE FRACTION OF DRV STACK GAS
FMO * (100. - BHO) / 100.
100. - 13.7
FMD a — —— ........ i .863
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GC1
MD a (PC02 • .44) * (P02 * .32) * (PN2 * PCO) * .28
MD a ( 4.20*44/100) * (10.5*32/100) * ((85.3* .0) * 28/100 = 29.09
MOLECULAR HEIGHT OF STACK GAS
MMS a MD • (1. • (BHO/100)) * 18. * (BHO/100)
MHS = 39.09* (1. -(13.72/100)) * 18. * (13.72/100) s 27.57
-------
STACK SAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SQRT(VM * (TS » 460.))
VS • 65.49 * CP • DELP / (SORT(MMS • PS) • PNTS)
VS o 85.49 * .84 • 84.631 / tSORTC 37.57 • 29.31) • 12. x 17.85 FP3
STACK 6AS VOLUMETRIC FLOM AT STACK CONDITIONS
OS s VS • AS * 3600/144
OS * 17.85 * 7466. 3600/144 • 3331033. ACFH
STACK GAS VOLUMETRIC FLOM AT STANDARD CONDITIONS
QSSTD • 17.647 •OS • PS •"UT- (BHO/100)) / (TS » 460.)
17.647 * 3331033. * 29.21 * (1. • (13.72/100))
OSSTD « ---------———- ——.——--——--— — - — - . z 1489327. SCFH
( 535. * 460.)
PERCENT ISOKINETIC
>
(Jn ISO * (305.5B«(TS+460.))*((0.002669*VLC)+(VM«Y«(PB+(PM/13.6))/(TM+460.)))/(TT*V3»PS*DN*DM
(30S.S8*( 535.4460.))*((0.002669* 1B9.)*( 57.227*1.003*t 29.30«( .620/13.6))/( 71.+460.)))
ISO • — ——————————————— — • t 113.40 PkRCENT
120. • 17.85 • 29.21 * .397 * .397
PARfiCULAfE LOADING --"EPA METHOD 5 (AT"STANDARD CONDITIONS)
C3 • 0.001 * MN * IS.43 / VMSTD
CS * 0.001 * .0 • 15.43 / 55.996 » .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR « CS * OSSTD / (15.43 • 453.6)
PMR • .000 * 1489327.7 (15.43 * «53.6) I .00
-------
Run No. ?.l
Sample volume =1.59 m3.56.QQ scf
Example calculations
CS (Part) =183.1/1.59 = 115.1 mq/m3
CS (Part) = 0.001 x!83.1 x 15.43/56.00 = 0.050 qr/dscf
CS (S02) =1370 /I.59 = 861.ana/m3
=861.6 x 24.06/64 = 3?4 ppm
= 0.001 x 1370 x 15.43/56.00 =0.377 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
183.1
61.6
84.2
1370
741 a
3 Concentration,
mg/m
115.2
38.7
53.0
861.6
466.0
gr/dscf
0.050
0.017
0.023
0.377
0.204
ppm
324
114
Hydrogen peroxide contaminate.
A-54
-------
FIELD DAT*
I
Uv
Ul
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PART/H2S04/S02
OPERATOR BRUFFEV
AMBIENT TEMP. (DEC. F) 69.
BAR. PRESS. (IN. HG) 29.30
STATIC PRESS, (IN. H20) •1.20
FILTER NUMBER(S) 35300013
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .B<»
THERM. NO.
LEAKAGE .000 CFM 9 S.O IN.HG
METER CALIB. FACTOR 1.044
READ I RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INlf
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
SO.O
90.0
100.0
110.0
120.0
TIME
(24-HR
ft f\f*tt \
CLUCK J
1558
1408
1418
1428
1438
1448
1458
1508
1518
1528
1538
1548
1558
READING
(CU.FT.)
961.498
965.910
970.265
974.650
979.000
983.345
987.710
992.070
996.400
.720
5.090
9.420
13.753
HEAD
(IN.H20)
.
.050
.050
.050
.050
.050
".050
.050
.050
.050
.050
.050
~ .050
DIFFERENTIAL
(IN.
DESIRED
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
H20)
ACTUAL
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
.62
STACK
TECP
(DtG.F)
573.
524.
532.
540.
543.
555.
568.
513.
S26.
536.
541.
559.
DATE 10/27/81
HUN NUMBER 2*2
PROBE LENGTH ft TYPE 4* HEATED GLASS
NOZZLE 2-2 : l.U. .397
ASSUMED MOISTURE 12.0
SAKPLE BOX NUPBEH
MtTER BOX NUHBER F10
ftTER HEAD OIFF. 1.80
C FACTOR .06
PROBE HEATER SETTING 25U.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .15
DHY GAS METER PUKP SAMPLE IMPINGER
TEMP
(DEG
INLET
71.
71.
73.
76.
77.
78.
78.
77.
78.
78.
77.
74.
.F)
OUTLET
72.
71.
72.
72.
72.
73.
73.
73.
72.
73.
72.
71.
VACUUM
(IN.HG)
.0
.0
.0
.5
.0
.0
2.0
2.0
2.4
2.5
2.5
2.6
BOX TEMP
(OEG.F)
268.
262.
262.
254.
264.
265.
267.
265.
262.
263.
256.
263.
TEMP
(OEG.F)
48.
47.
49.
51.
50.
50.
50.
50.
53.
54.
56.
52.
TOTALS
AVERAGE
120.0
52.255
.62
.62 543.
76.
72.
1.7 263.
51.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
2-2
NO.l COKE BATTERY OUTLET
I
Ul
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
DN
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
10/27/61
1356
1556
120
12
1
.0
.044
.397 IN
.••*
.62 IN-H20
METRIC UNITS
10/27/81
1358
1558
120
12
1
10
15
.0
.044
.1
.84
.7
CM
CM-
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTO VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENt MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENt 02 BY VOL;, D«t
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR MT-DffY STACK GAS
MMS MOLECULAR MT-STACK GAS
52.255 CU-FT
73.9 F
52.914 SCF
169.2
7.964 SCF
1.480 CU-M
23.3 C
1.498 SC^
169.2
.226 SO
13.06
.669
4.20
10.50
.00
65.30
29.09
27.64
13.08
.869
4.20
10.50
.00
85.30
29.09
27.64
-------
PB
PSI
PS
TS
VS
AS
OSSTO
OS
ISO
MN
CS
PMR
*
1
en
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOM RATE* DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
FILTERABLE PART
MG. EPA 5
FILTERABLE PART
FILTERABLE PART
EMISSION RATE
6* DEC F, 29.92 IN.H6.
. . . - . _ „ ._ _
29.30 IN-HG
"1.20 IN-H20
29.21 IN-HG
543. F
~17.9 FPS
7466. SO-IN
1492594. SCFH
3339539. ACFH
106.9
.0
.0000 GR/DSCF*
.000 LB/HR
.
700.22 *M-HG
-30.08 HH-H20
741.96 CM-HG
284. C
5.5 VPS
4.817 SO-M
42266. 3CMH
94566. »CVH
106.9
.0
.000 HG/OSC
.00 KG/HH
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 2-2
NO.l COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.607 « VM • Y • (PB « PM / 13~i6)) / (TM * 060.)
17.647 • 52.255 * 1.004 • ( 29.30 «• .620 / 13.6)
VMSTO * ——————— — — ——— ———- — ---- r 52.9la DSCF
( 74. «• 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VWC * .04707 • VLC
VHC » .04707 * 169. * 7.96 SCF
PERCENT MOISTURE IN STACK GAS
BNO « (100. • VKC) / (VMSTD * VWC)
100. * 7.96
BMO • —— ———— s 13.08 PERCENT
jp 58.914 * 7.96
I ... .... .. .... ...
Ul
oo
MOLE FRACTION OF DRY STACK GAS
FMD « (100. • BNO) / 100.
100. - 13.i
FMD » ————————— * .869
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO * (PC02 • .44) * (P02 * .32) » (PN2 «• PCO) * .28
MD = ( 4.20*44/100) » (10.5*32/100) * ((85.3* .0) * 28/100 = 29.09
MOLECULAR WEIGHT OF STACK GAS
MNS « MD * (1. - (BMO/100)) * 18. * (BNO/100)
MNS * 29.09* (1. -(13.08/100)) » 18. * (13.08/100) » 27.64
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP • SUM. OF THE SORMVH * (TS » 460.))
VS * 85.19 • CP • DELP / (SORT(MNS * PS) * PNTS)
VS > 85.49 * .84 • 84.956 / (SQRT( 37.64 • 29.21) * 12. - 17.89 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS » VS * AS * 3600/144
OS * 17.89 • 7466. 3600/144 * 3339959. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD * 17.647 * OS • PT~* (1. - (BMO/100)) / (TS * 460.)
17.647 * 3339559. * 29.21 * (1. - (13.08/100))
OSSTD * — ——— —— —— = 1«9259
Ui (305.5SM 543.+460.))*((0.002669»~ 169.)V( 52.255*1.044*( 29.30+( .620/13.6))/( 70.+060.)))
VD iso • ——————................................................—...............—..... ....... s 106.92 PEHCEM
120. • 17.89 • 29.21 * .397 * .397
PARTICULATE LOADING -- EPA METHOD s (AT STANDARD CONDITIONS)
CS * 0.001 • MN • 15.43 / VMSTD
CS • 0.001 * .0 * 15.43 / 52.914 a .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR s CS * QSSTD / (15.43 * 453.6)
PMR * .000 * 1492594. / (15.43 * 453.6) = .00
-------
Run No. 2.2
o
Sample volume = 1.50 m . 52.9 scf
Example calculations
CS (Part) =149.2/1.50 = 99.5 mq/m3
CS (Part) = 0.001 x 149.2x 15.43/52.91 = 0.044 qr/dscf
CS (S02) = 1720/ 1.50=n46.7mo/m3
=1146.7 x 24.06/64 = 431 ppm
= 0.001 x!720 x 15.43/52^9J_ = n.sm gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
149.2
24.8
n.o
0.0
1720
16.0
, Concentration,
mg/m
99.5
16.5
0.0
0.0
1146.7
10.7
gr/dscf
0.044
0.007
0.0
0.0
0.502
0.005
ppm
431
3
A-60
-------
FIELD DATA
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 2-3-M8-400
OPERATOR CLARKE
AMBIENT TEMP. (DEG.F) 69.
BAR. PRESS. (IN.HG) 29.30
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530057
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 2.0 IN.HG
METER CALIB. FACTOR .992
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
f*l f\f* V 1
UL.UCR J
1355
1405
1415
1425
1435
1445
1455
1505
1515
1525
1535
1545
1555
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE
DIFFERENT
(IN.H20)
1AL
STACK
TEMP
(DEG.F)
DESIRED ACTUAL
472.072
476.400
480.900
485.375
489.689
494.120
498.525
502.915
507.405
511.695
516.198
520.470
524.984
.050
.050
.050
.050
.050
,050
.050
.050
.050
.050
.050
.050
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
525.
519.
530.
537.
535.
543.
565.
511.
522.
534.
534.
553.
DATE 10/27/81
RUN NUMBER 2-3
PROBE LENGTH ft TYPE 5 FT GLASS HEATED
N02ZLE 2-3: I.D. .398
ASSUMED MOISTUHE 12.0
SAMPLE BUX NUMBER
PETER BUX NUMBtH FBI
KETEH HEAD 01FF. 1.87
C FACTON .88
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
HEFERENCE PRESS. DIFF. .15
DKY GAS METER
TEMP
(DEG.F)
INLET OUTLET
64. 60.
66. 60.
JO. 60.
72. 61.
74. 62.
76. 64.
76. 62.
76. 64.
76. 62.
76. 63.
76. 65.
78. 64.
PUMP
VACUUM
(IN.HG)
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
SAMPLE
BOX TEMP
(DEG.F)
300.
365.
389.
365.
406.
383.
416.
393.
404.
409.
426.
414.
IMPINGEK
TEMP
(DEG.F)
52.
42.
52.
52.
54.
54.
56.
56.
52.
52.
58.
58.
TOTALS
AVERAGE
120.0
52.912
,60
.60 534.
73.
62.
2.0 369.
53.
-------
PARTICIPATE FIELD DATA S RESULTS TABULATION
PLANT* NAME AND ADDRESS ~ TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
2-3
COKE OVEN OUTLET
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
10/27/61
1355
1555
120
12
.0
.992
.398 IN
.64
.60 IN-H2U
METRIC UNITS
10/27/61
1355
1555
120.
12
*
10.
•
15.
0
992
1
84
2
»«
PM-
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPIN6ERS AND SILICA GEL,ML,
VMC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
6*0 PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRV GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BriniL.T DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR MT-DRV STACK GAS
MNS MOLECULAR MT-STACK GAS
52.912 CU-FT
1.496 CU-M
67.
51.
175.
6.
13.
•
4.
10.
•
65.
29.
27.
6 F
499 SCF
q
021 SCF
40
665
20
50
00
30
09
60
19.
1.
170.
•
13.
•
4.
to.
•
85.
29.
27.
9
458
4
227
48
865
20
50
00
30
09
60
C
SCP
SC*
-------
PB BAROMETRIC PRESSURE
P8I STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
QSSTD STACK FLOW RATE. DRY*
OS ACTUAL STACK FLO* RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 DEC F, 29.92 IN.H6.
39.30 IN-HG
-i.20 IN-H20
29.21 IN-HG
534. F
~if.e FPS
7466. SO-IN
1493373. SCFH
3338048.
103.5
.0
ACFH
.0000 GR/DSCF*
.000 LB/HH
744.22 MM-HG
-30.48 *M-H20
741.98 KH-Mli
279. C
5.4 KPS
4.817 30-M
42288. 3CCH
94240.
103.5
.0
.000
.00 KG/HR
I
CTl
U)
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 2-3
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.647 * VM * Y * (PB » PM / IS. 6)) / (TM » 460.)
17.64? • 52.912 * .992 • ( 39.30 » .600 / 13.6)
VMSTD « — --- ——————. ----- ....... ------------------ a 51.
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP » SUM. OF THE SQRT(VH * (TS * 460.))
VS * 85.49 * CP * OELP / (SORTCMHS * PS) * PNTS)
VS * 85.49 * .84 * 84.596 / (SORT( 27.60 • 29.21) • 12. r 17.83 FP3
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
03 « VS • A3 * 3600/144
OS * 17.83 • f466. 3600/144 » 3328042. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD * 17.647 • 03 * P3 * (1. - (BNO/100)) / (TS » 460.)
17.647 * 3328042. * 29.21 * (1. - (13.48/100))
OSSTO * ....—............................................ s 1493373. SCFH
( 534. * 460.)
PERCENT ISOKINETIC
> ISO • (305.58*(TS+460.))*U0.002669*VLC)«(VM*V*(PB+(PM/13.6))/(TM«460.)))/(TT«V9*PS«DN*DN)
I
'" (30S.M«( 534.*«60.))«C(0.002669
-------
Run No. 2.3
Sample volume =_l.A£m ,__51_5Q_scf
Example calculations
CS (Part) =46.3 /1.46= 31.7 mq/m3
CS (Part) = 0.001 x46.3 x 15.43/51.50=0.014 qr/dscf
CS (S02) = 1700/1.46=n64.3ng/m3
= 1164.3x 24.06/64 =438 ppm
= 0.001 x1700 x 15.43J51.50 = 0.50 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
46.3
12.2
16.7
1700
53.0
3 Concentration,
mg/m
31.7
8.3
11.4
1164.7
36.3
gr/dscf
0.014
0.004
0.005
0.509
0.016
ppm
438
9
A-66
-------
FIELD DAT*
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 2-4-M8-400
OPERATOR CLARKE
AMBIENT TEMP. (DEC. F) . 69.
BAR. PRESS. UN. HS) 29.30
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530062
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 8 2.0 IN.HG
METER CALIB. FACTOR 1.016
READ * RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT TIME
NO. (MIN.)
INIT 0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
TIME
(24-HR
ft np v i
(*LUt n i
ms
1408
1418
1428
1438
1448
1458
1508
1518
1528
1538
1548
'1558 ~
READING
(CU.FT.)
898.35)
902.665
906.900
911.186
915.762
919.670
924.085
928.200
932.712
936.920
940.920
945.776
949.848
HEAD
(IN.H20)
• • - - -
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
DIFFERENTIAL
(IN.
DESIRED
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
H20)
ACTUAL
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
.60
STACK
TEMP
(DEG.F)
573.
524.
530.
539.
543.
555.
566.
514.
525.
536.
541.
559.
DATE 10/27/81
NUN NUMBER i-n
PRUBE LENGTH « TYPE 6 FT GLASS HEATED
NU22LE 2-4t I.D. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER F
METER BOX NUMBER FBS
METEH HEAD DIFK i.t»6
C FACTOR .68
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
tfEFEKENCE PRESS. DIFF. .75
DKY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM
(DEG
I&LET
68.
69.
72.
74.
76.
78.
78.
78.
78.
78.
78.
62.
.F) (IN.HG)
OUTLET
69.
69.
70.
70.
70.
72.
72.
72.
72.
72.
72.
74.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(DEG.F)
405.
369.
386.
430.
373.
394.
392.
394.
422.
413.
450.
418.
TEMP
(OEG.F)
42.
38.
40.
42.
46.
48.
46.
44.
42.
44.
46.
48.
TOTALS
AVERAGE
120.0
51.495
.60
.60 542.
76.
71.
1.0 404.
44.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
2-4
COKE OVEN OUTLET
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
I VM
CO
TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
ENGLISH UNITS
10/27/81
1358
1558
120.0
12
1.016
.397 IN
. ..••«
.60 IN-H20
51.495 CU-FT
T3.5 F
50.787 SCF
METRIC UNITS
10/27/81
1358
1558
120.0
12
1.016
10.1
.84
15.2
1.458
23.0
1.438
KM
CM-H20
CU-M
C
SCK
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GELrML.
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
8Mb ~ PERCENT MOISTURE BT VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BT VOL.r DRY
P02 PERCENT 02 6T VOL.; DRY
PCO PERCENT CO BY VOL.* DRY
PN2 PERCENT N2 BY VOL.r DRV
MO MOLECULAR NT-DRY STACK GAS
MMS MOLECULAR XT-STACK GAS
156.1
7.348 SCF
156. 1
.208 SC»
12.64
.874
4.20
10.50
.00
05.30
29.09
27.69
12.64
.874
4.20
10.50
.00
85.30
29.09
27.69
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
QSSTO STACK FLO* RATE* DRY*
OS ACTUAL STACK FLOM RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 6* DEC Ft 29.92tN.H6.
29.30 IN-HG
•1.20 IN-H20
29.21 IN-HG
542. F
if.9 FPS
7466.
1499060.
3336176.
102.2
.0
SO-IN
SCFH
ACFH
.0000 GR/DSCF*
.000 LB/HH
Taa.22 KM-HG
-30.48 HM-H20
741.98 MM-HG
283. C
5.4 HP8
4.817 SO-M
42449. SCHH
94471. ACMH
1U2.2
.0
.000 HG/OSCP
.00 KG/HR
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 2-4
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 • VM • T • (PB » PM / 13.6)) / (TM » 460.)
17.647 • 51.495 * 1.016 • ( 29.30 * .600 / 13.6)
VMSTO * — — — — — -------- ..... --- . --- . -------------------- - 50.787 USCF
I 73. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC m .04707 • VLC
VHC • .04707 * 156. » ~7.3S SCF
PERCENT MOISTURE IN STACK GAS
BMO a (100. * VMC) / (VMSTO * VHC)
100. • 7.35
——————— z 12.64 PERCENT
50.787 * 7.35
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - BMO) / 100.
loo. - it.*
FMD m —————— x .874
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MD • (PC02 • .44) «• (P02 • .32) * (PN2 * PCO) * .28
MO = ( 4.20*44/100) * (10.5*32/100) » ((85.3* .0) • 28/100 = 29.09
MOLECULAR HEIGHT OF STACK GAS
MHS s MD * (1. - (BMO/100)) » 18. • (BHO/100)
MMS « 29.09* (1. -(12.64/100)) * IB. * 112.64/100) r 27.69
-------
STACK CAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SORTtVH * (TS * 460.))
VS a 85.49 * CP • DELP / ISQRTtMMS * PS) * PNTS)
VS = 65.49 * .84 * 84.945 / (SORT( 27.69 * 29.21) * 12. a 17.87 FP3
STACK CAS VOLUMETRIC FLOM AT STACK CONDITIONS
OS > VS * A3 * 3600/144
OS a 17.87 « 7466. 3600/104 m 3336176. ACFH
STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD « 17.647 • OS • PS • U. - (BMO/lOO)) / (TS * 460.)
17.647 * 3336176. * 29.21 * (1. - (12.64/100))
OSSTD a ————————.—-————- — - — ... 3 1499060. SCFH
( 542. * 460.)
PERCENT ISOKINETIC
> ISO • (305.58*(TS»460.))«((0.002669«VLC)*lVM*r*(PB*(PM/13.6))/(TM*460.)))/(TT«VS*PS«DN*DN)
^ (305.58«( 542.*460.))*((0.002669i- I56.)+( 51.495*1.016*( 29.30*1 .600/13.6))/( 73.4460.)))
ISO » ————— ........ ................. . .. .. . . . 102.18 PEHCENT
120. • 17.87 * 29.21 * .397 * .397
PARTICIPATE LOADING "EPA METHOD 5 (AT STANDARD CONDITIONS)
CS a 0.001 • MN • 15.43 / VMSTD
CS • 0.001 * .0 * 15.43 / 50.787 * .000 GR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR • CS * OSSTD / (15.43 * 453.6)
PMR • .000 * 1499060. / (15.43 * 453.6) = .00
-------
Run No. 2.4
Sample volume = 1.44m3r 50.79scf
Example calculations
CS (Part) =61.3 /1.44 =42.6 mq/m3
CS (Part) = 0.001 x 61.3 x 15.43/50.79 = 0.019 qr/dscf
CS (S02) = 1610/1.44=1118.Qng/m3
J118.0 x 24.06/64 =420 ppm
= 0.001 x!610 x 15.43/50.79 = 0.489 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2$04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
61.3
14.4
19.7
1610
19.6
o Concentration,
mg/m
42.6
10.0
13.7
1118.0
13.6
gr/dscf
0.019
0.004
0.006
0.489
0.006
ppm
420
3
A-72
-------
FIELD DAT*
I
^1
OJ
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE OVEN STACK
SAMPLE TYPE METHOD 5-250
OPERATOR 00
AMBIENT TEMP.(DEG.F) 63.
BAR. PRESS. (IN. H6> 29.03
STATIC PRESS. (IN. H20) -1.20
FILTER NUHBER(S) 3530000
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .012 CFM 9 7.
METER CALIB. FACTOR 1.033
READ S RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INIT
SAMPLE CLOCK
TIME
(MIN.
0
10.0
20.0
30.0
40.0
50.0
'60.0
70.0
ao.o
90.0
100.0
110.0
120.0
TIME
) (24-HR
ft nr» M i
CLUCK 1
1424
1434
1444
1454
1504
1514
~ 1524
1534
1544
1554
1604
1614
1624
GAS METER
READING
(CU.FT.)
645.051
649.460
653.770
658.110
662.460
666.820
671.190
675.560
679.940
684.320
686.710
693.140
697.556
VELOCITY
HEAD
(IN.H20)
.057
.057
.057
.057
.057
.057
.057
.057
.057
.057
.057
,05f
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIREU
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
H20)
ACTUAL
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
STACK
TEfP
(OEG.F)
499.
499.
099.
099.
099.
099.
099.
099.
099.
099.
099.
099.
DATE 10/27/81
HUN NUMBER 2-5
HHOBE LENGTH 8 TYPE 6* GLASS
NOZZLE 6-1101 I.U. .377
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBEH FBO
METER HEAD 01FF. 1.88
C FACTOR .92
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
HEFENENCE PRESS. DIFF. .17
DRY GAS METER
TEMP
(OEG.F)
INLET OUTLET
67. 66.
68. 66.
1i. 67.
70. 68.
77. 69.
76. 70.
79. 71.
00. 72.
SO. 73.
»0. 73.
80. 73.
79. 73.
PUPP
VACUUM
(IN.HG)
3.7
.7
.0
.1
.2
.4
.5
.8
5.0
5.0
5.7
5.7
SAMPLE
BOX TEMP
(OEG.F)
234.
271.
271.
238.
252.
262.
208.
271.
205.
252.
275.
261.
IPPINGER
TEMP
(DEG.F )
so.
50.
50.
08.
06.
48.
08.
50.
50.
50.
50.
48.
TOTALS
AVERAGE
120.0
52.507
.63
.63 099.
76.
70,
0.6 257.
49.
-------
PARTICIPATE FIELD DATA S RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEA* LEADER
REPUBLIC STEEL CLEVELAND DO
TEST
2-5
COKE OVEN STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
> VM
1
•* TM
VMSTD
VLC
VMC
BNO
FMD
PC02
P02
PCO
PN2
MO
MHS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 8V VOL., DRV
PERCENT CO BY VOL., DRV
PERCENT N2 BY VOL., DRY
MOLECULAR HT-ORY STACK GAS
MOLECULAR MT-STACK GAS
ENGLISH UNITS
10/27/81
1424
1624
120.0
12
1.033
.377 IN
.84
.63 IN-H20
52.507 CU-FT
T3.1 F
52.922 SCF
ns.s
8.261 SCF
13.50
.865
4.20
10.50
.00
85.30
29.09
27.59
METRIC UNITS
10/27/81
1424
1624
120.0
12
1.033
9.6
.84
16.0
1.487
22.8
1.499
175.5
.234
13.50
.865
4.20
10.50
.00
85.30
29.09
27.59
MM
MM-H20
CU-M
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRESf ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLOW RATE* DRY*
OS ACTUAL STACK FLOH RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 OEG F, 39.93 IN.HG.
29.43 IN-HG
-1.20 IN-H20
29.34 IN-HG
499. F
18.7 FPS
7066. SO-IN
1636567. SCFH
3482787.
108. 8
.0
ACFH
.0000 GR/OSCF*
.000 LB/HR
707.52 MM-HG
-30.48 KM-H20
745.28 PM-HG
259. C
5.7 *P3
4.817 3Q-M
46059. 3CfH
98622. ACMH
108.8
.0
.000
.00 KG/HR
I
•~J
Ul
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 2-5
COKE OVEN STACK
VOLUME OP DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO » (17.64f • VM * Y * (PB V PM / U.6)) / (TM «• 460.)
17,647 * 52.507 • 1.033 * ( 29.43 * .630 / 13.6)
VMSTD « ————————.———.——. — ... — .. — .. 3 58.S22 OSCF
I 73. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC » .04707 * VLC
VMC « ,04707 * If 6. • 8.26 SCF
PERCENT MOISTURE IN STACK GAS
BHO « (iOO. • VMC) 7 (VMSTO * VWC)
100. * 6.26
BHO « — — --- — — ----- — ---- — a 13.50 PERCENT
> 52.922 * a. 26
I
~j ......
CTi
MOLE FRACTION OF DRV STACK GAS
FMD * (100. • BMO) / 100.
100. - Il.f
FMD * —.———.——— --- r .865
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD * (PC02 * .44) * (P02 * .32) » (PN2 * PCO) * .28
MD a ( 4.20*44/100) + (10.5*32/100) * ((85.3* .0) * 28/100 « 29.09
MOLECULAR MEIGHT OF STACK GAS
MM 3 a MD * (1. - (8MO/100)) * 18. * (BHO/100)
MMS * 29.09* (1. -(13.50/100)) » 18. * (13.50/100) » 27.59
-------
STACK 6A3 VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SQRT(VH * (TS * 460.))
VS * 85.49 • CP • OELP / (SORT(MMS • PS) * PNTS)
V3 = 8S.49 • .84 * 88.721 / (3URT( 27.59 • 29.34) * 12. s 16.66 FPS
STACK CAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS « VS * AS * 3600/144
OS * 18.66 • 7466. 3600/144 • 3482787. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTO * 17.647 * OS • PS * (1. - (BMO/100)) / (TS » 460.)
17.647 * 3482787. * 29.34 * (1. - (13.50/100))
OSSTD * — -—-.—————..— — — ——.. —.- e 1626567. SCFH
( 499. «• 460.)
PERCENT ISOKINETK
> ISO * (305.58*(TS+460.))M(0.002669*VLC)«(VH*V*(PB*(PM/13.6))/(TM+460.)))/(TT*V3*PS*ON*DN)
I
-J (305.58M 499.*460.))*((0.002669* 176.)*{ $2.507*1.033*( 29.03*1 .630/13.6))/( 73.+460.)))
ISO « ————————— — ..... . .. > 108.62 PEHCEM
120. * 18.66 * 29.34 • .377 * .377
PARTICIPATE LOADING"-- EPA METHOD 5 (AT STANDARD CONOltlONS)
CS « 0.001 • MN • 15.43 / VMSTD
CS s 0.001 * .0 « 15.43 / 52.922 = .000 GR/DSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR « CS * OSSTD / (15.43 * 453.6)
PMR « .000 * 1626567. / (15.43 * *53.6) * .00
-------
Run No. 2.5
Sample volume = 1.50 m . 52.92 scf
Example calculations
CS (Part) =90.9/1.5 = 60.6 mq/m3
CS (Part) = 0.001 x90-9 x 15.43/52.92 = 0.026 qr/dscf
3
CS (S02) = / = mg/nr
= x 24.06/ = ppm
= 0.001 x x 15.437
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sul f uric acid mist
As H2$04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
90.9
34.0
30.7
29.2
27.7
22.5
0.0
0.0
68.2
4.8
44.3
3 Concentration,
mg/m
60.6
22.7
20.5
19.5
18.5
15.0
0.0
0.0
45.5
3.2
29.5
gr/dscf
0.026
0.010
0.009
0.008
0.008
0.006
0.000
0.000
0.020
0.001
0.013
ppm
A-78
-------
FIELD DATA
i
-o
vo
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN STACK
SAMPLE TYPE METHOD 6-600
OPERATOR 00
AMBIENT TEMP. (DEG.F) 63.
BAR. PRESS. (IN.HG) 29.43
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530212
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .64
THERM. NO.
LEAKAGE .000 CFM 8 21.7 IN.HG
METER CALIB. FACTOR .962
READ • RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INlt
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
60.0
90.0
CLOCK
TIME
(24-HR
1419
1429
1439
1449
1459
1509
1519
1529
1539
1549
GAS METER
READING
(CU.FT.)
141.627
149.070
156.460
163.870
170.840
177.430
163.760
169.600
195.720
201.620
VELOCITY
HEAD
(IN.H20)
.057
.057
.057
.057
.057
.057
.057
.057
.057
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.66
.66
.68
.68
.68
.66
.68
.68
.68
H20)
ACTUAL
.90
.90
.90
.60
.49
.36
.28
.15
.13
STACK
TEMP
(OEG.F)
499.
499.
499.
499.
499.
499.
499.
499.
499.
DATE 10/27/61
HUN NUMBER 2-6
PROBE LENGTH S TYPE 4' QUARTZ
NOZZLE ! 1.0. .590
ASSUMED MOISTURE 11.0
SAMPLE BUX NUMBER
METER BOX NUMBER FB8
ME1EH MEAD OIFF. 1.91
C FACTOH .94
PROBE HEATER SETTING 600.
HEATER BUX SETTING t>oo.
DEFERENCE PRESS. OIFF. .03
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
63. 62.
66. 62.
70. 62.
72. 63.
71. 63.
70. 64.
69. 64.
66. 63.
68. 63.
PUMP
VACUUM
(IN.HG)
7.2
6.6
12.6
19.8
20.5
20.6
21.0
21.4
21.4
SAMPLE
BOX TEMP
(OEG.F)
617.
564.
596.
619.
567.
576.
566.
616.
635.
IMPINGER
TEMP
(DEG.F)
42.
44.
50.
60.
58.
56.
56.
54.
50.
TOTALS
AVERAGE
90.0
59.993
3.66
1.55
499.
69.
63.
17.1
600,
52.
-------
PARTICUIATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO
TEST
2-6
COKE OVEN STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1 VM
00
o
TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
ENGLISH UNITS
10/27/81
1509
90.0
9
.982
.590 IN
.80
1.55 IN-H20
59.993 CU-FT
65.7 F
58.020 SCF
METRIC UNITS
10/27/81
1019
1509
90.0
9
.982
15.0
.80
39.3
1.699
18.7
1.650
I'M
MM-H20
CU-M
C
SCK
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRV
P02 PERCENT 02 B? VOL., DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRV
MD MOLECULAR NT-DRY STACK GA9
MWS MOLECULAR MT-STACK GAS
7.056 SCF
109.9
.200 SO
10.78
.892
0.20
10.50
.00
85.30
29.04
27.90
10.78
.892
0.20
10.50
.00
85.30
29.09
27.90
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK 6AS
PS STACK PRES, ABS.
TS AVERA6E STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLON RATE, DRY*
os ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 29.92 iN.HG.
29.43 IN-HG
•1.20 IN-H20
29.34 IN-HG
499. F
18.6 FPS
7466. SO-IN
1666717. SCFH
5463857. ACFH
63.7
.0
.0000 GR/DSCF*
.000 LB/HR
747.52 fM-HG
•30.46 CM-H20
745.28 CM-HG
259. C
5.7 *P3
4.617 SO-M
47253. SC»»H
96066. ACHH
63.7
.0
.000 PG/DSCP
.00 KG/HR
I
00
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 2-6
COKE OVEN STACK
VOLUME OF DRY 6A9 SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 * VM * T * (PB » PM / 13.6)) / (TM * 460.)
17.647 * 59.993 • .982 * ( 29.43 * 1.548 / 13.6)
VMSTD « ——————-———.—...........—........... 3 56.424 OSCF
I 66. «• 460.)
VOLUME Of MATER VAPOR AT STANDARD CONDITIONS
VMC « .04707 • VLC
VHC • .04707 * ISO. » 7.06 SCF
PERCENT MOISTURE IN STACK GAS
BMO » (100. • VMC) '/ (VMSTD » VMC)
100. * 7.06
BMO « —— ——— ...... 3 10.78 PERCENT
;> 58.424 * 7.06
I
oo "" " ' "
NJ
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - BMO) / 100.
100. - 10.8
FMD » ——.———.—— s .892
100.
AVERAGE MOLECULAR HEIGHT OF DRV STACK GAS
MD « (PC02 * .44) » (P02 * .32) » (PN2 • PCO) * .28
MD * ( 4.20*44/100) * (10.5*32/100) * ((85.3* .0) * 28/100 s 29.09
MOLECULAR MEIGHT OF STACK GAS
MMS * MO * (1. - (BMO/100)) » 18. * (BMO/100)
MMS a 29.09* (1. -(10.76/100)) * 18. * (10.78/100) s 27.90
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE SORHVH * (TS * 060.))
VS * 65. 49 • CP * OELP / (SORTCMNS * PS) * PNTS)
VS > 95.49 • .84 * 66.541 / (SORT( 27.90 * 29.34) •
9. a 16.56 FPS
STACK 6AS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS • IB. 56 * 7466. 3600/144 « 346S657. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD * 17.647 * OS • PS * (1. • (BMO/100)) / (TS + 460.)
17.647 • 3463657. • 29.34 * (1. - (10.76/100))
—————————— — ............. ---- ......
( 499. » 460.)
OSSTO »
1666717. SCFH
S
PERCENT ISOKINETIC
ISO • (305.58*(TS*460.) )«((0.002669*VLC)»(VM*Y*(PB*(PH/13.6) ) /
-------
Run No. 2.6
Sample volume = I-65 m , 58.42 scf
Example calculations
CS (Part) =39.5/1.65 = 23.9 mo/m3
CS (Part) = 0.001 x 39-5 x 15.437 58.42= 0.010 qr/dscf
CS (S02) = 1940/1.65 =1175.8mo/m3
=1175.8X 24.06/64 = 442 pDtT1
= 0.001 xJiiLx 15.43/58.42 = 0.512 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H£S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
39.5
2.6
3.5
1940
157
3 Concentration,
mg/m
23.9
1.6
2.1
1175.8
95.7
gr/dscf
0.010
0.001
0.001
0.512
0.041
ppm
442
23
A-84
-------
FIELD DATA
I
00
Ul
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION N01 COKE BATTERY OUTLET
SAMPLE TYPE PART/302/H2SU4
OPERATOR BRUFFEY
AMBIENT TEMP. (DEG.F) 58.
BAR. PRESS. (IN. HG) 29.78
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3930093
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 3 3.0 IN.HG
METER CALIB. FACTOR 1.003
READ ft RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
9
10.0
20.0
30.0
• 0.0
50.0
60.0
70.0
ao.o
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
f i ncK i
vLUtK;
955
1005
1015
1025
1035
1045
1055
1105
1115
1125
1135
lias
1155
EVERT 10. 0
GAS METER
READING
(CU.FT.)
777.764
783.020
788.000
793.070
798.540
803.570
808.620
813.670
818.720
823.350
828.440
833.520
838.555
MINUTES
VELOCITY
HEAD
(IN.H20)
.065
.060
.060
.070
.060
.060
.060
.060
.050
.060
.060
.060
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.80
.73
.73
.87
.73
.73
.73
.73
.61
.73
.73
.73
H20)
ACTUAL
.80
.73
.73
.87
.73
.73
.73
.73
.61
.73
.73
.73
STACK
TEMP
(DEG.F)
546.
515.
525.
536.
531.
550.
558.
517.
528.
539.
529.
545.
DATE 10/28/81
RUN NUMBER 3-1
PROBE LENGTH ft TYPE 5* HEATED GLASS
M022LE t I.U. .398
ASSUMED MUISTUHE 12.0
SAMPLE BOX NUMBER U
METEN BOX NUMBtk FB2
HETEH HEAD OIFF. 1.76
C FACTOR .86
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
HEFERENCE PRESS. DIFF. .15
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
54. 55.
56. 55.
58. 56.
61. 55.
62. 56.
62. 56.
63. 56.
64. 57.
6«. 57.
64. 57.
64. 57.
64. 57.
PUMP
VACUUM
(IN.HG)
2.0
2.0
2.5
2.0
2.5
2.5
2.5
2.5
3.0
3.0
3.0
3.0
SAMPLE
BOX TEMP
(DEG.F)
160.
228.
251.
239.
248.
248.
247.
245.
242.
245.
241.
234.
IMPINGEH
TEMP
(OEG.F)
44.
44.
43.
4a.
43.
44.
4«.
46.
44.
42.
44.
43.
TOTALS
AVERAGE
120.0
60.791
.74
,74 535.
61.
56.
2.5 236.
44.
-------
PARTICULATE FIELD DATA » RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
3-1
NOI COKE BATTERY OUTLET
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
_CP
PM
1 VM
00
en
TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
10/28/81
953
1155
120.
12
1.
.
__._•
•
60.
58.
61.
0
003
398 IN
64
74 IN-H20
791 CU-FT
8 F
683 SCF
METRIC UNITS
10/26/81
955
1155
120
12
1
10
16
1
la
1
.0
.003
.1
.64
.T
.721
.9
.752
I'M
MM-H20
CU-M
C
SCM
AT STANDARD CONDITIONS*
VLC TOTAL H2«i COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
0MO PERCENT MOIfTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRY
P02 PERCENT 02 BY VOL., DRV
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL.* DRY
MD MOLECULAR HT-DPY STACK GA3
MMS MOLECULAR MT-STACK GAS
8.633 SCF
163.4
.244 SCN
12.24
.878
2.30
10.90
.00
86.80
28.60
27.48
12.24
.876
2.30
10.90
.00
66.80
26.80
27.48
-------
PB BAROMETRIC PRESSURE
P9I STATIC PRES OF STACK GAS
PS STACK PRES, AB9.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLOW RATE, DRY*
OS ACTUAL STACK FLO* RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 OEG F, 29.92 IN.HG.
29.78 IN-MG
•1.20 IN-M20
29.69 IN-HG
535. F
19.5 FPS
7466. SO-IN
1680373. SCFH
3635799.
110.5
.0
ACFH
.0000 GR/OSCF*
.000 LB/HR
756.ai MM-HG
-30.a8 KM-H2U
750.17 MM-HG
279. C
5.9 KPS
1.817 30-M
47583. SCI»H
102955. »CKM
110.5
.0
.000 KG/DSC^
.UU KG/HH
I
00
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 3-1
N01 COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO « (17.647 • VM • Y • (PB * PM / 13.6)) / (TM + 460.)
17.647 * 60.791 * 1.003 * ( 29.78 «• .736 / 13.6)
VMSTD • ——... . .. = 61.883 OSCF
I 59. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC » .04707 * VLC
VMC » .04707 * 103. s 6.63 SCF
PERCENT MOISTURE IN STACK GAS
BWO i'tiOO. • VWC) 7~(VMSTD * Vt«C)
too. • a.63
BNO * —.—— . .......... * 12.24 PERCENT
> 61.883 * 8.63
oo - —
CO
MOLE FRACTION OF DRY STACK GAS
FMD » (100. - BHO) / 100.
100. - 12.2
FMD « ——————......... c .878
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD * (PC02 • .44) 4 (P02 * .32) » (PN2 • PCO) * .28
MD a ( 2.30*44/100) * (10.9*32/100) + ((86.8* .0) « 28/100 = 28.80
MOLECULAR HEIGHT OF STACK GAS
MNS > MD * (1. - (BMO/IOO)) * 18. * (BMO/100)
MNS « 28.80* (1. •(12.24/100)) * IB. * (12.24/100) * 27.48
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE 3QRT(VH • ITS » 460.))
VS « 85.49 • CP • DELP / (SORT(MHS • PS) * PNTS)
VS > 85.49 • .84 • 92.979 / (SQRT( 27.48 • 29.69) • 12. = 19.«8 FP3
STACK GAS VOLUMETRIC FLOM AT STACK CONDITIONS
OS > VS • AS • 3600/144
OS * 19.48 • 7466. 3600/144 • 3635799. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD * 17.647 • OS • PS • (1. - tBMO/100)) / (TS * 460.)
17.647 • 3635799. * 29.69 • (1. - (12.24/100))
OSSTD » ———————————————............. = 1680373. SCFH
( 535. » 460.)
> PERCENT ISOKINETIC
I
^ ISO * (305.5B*(TS»460.))*((0.002669*VLC)*(VM*Y*(PB*(PM/13.6))/(TM*460.)))/(TT*VS*P3*ON*DN)
(30S.58*( 53S.+460.))*((0.002669* 183.)*( 60.791*1.003*( 29.78+( .738/13.6))/( 59.+060.)))
ISO » .-—-.—......... ......... ...... .... .. ... . ... . B 110.51 PERCENT
120. * 19.48 * 29.69 * .398 * .398
PARTiCULATE LOADING •• EPA METHOD 5 (AT'STANDARD CONDITIONS)
CS • 0.001 * MN * 15.43 / VM3TD
CS * 0.001 * .0 • 15.43 / 61.883 > .000 GR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PAR B CS * OSSTD / (15.43 • 453.6)
PMR * .000 • T6ad373. I (15.43 *"«53.6) * .00
-------
Run No. 3.1
Sample volume = 1.75m3f61.88 scf
Example calculations
CS (Part) =202.0/1.75 = 115.4 mq/m;
CS (Part) = 0.001 x202-0 x 15.43^-88 = 0.050 qr/dscf
CS (S02) = 1790 / 1.75 = 1022.4a/m3
=2022.8* 24.06/64 = 384ppm
= 0.001 x1790 x 15.43/Jit88_
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
202.0
70.4
96.2
1790
8.3
3 Concentration,
mg/m
115.4
40.2
55.0
1022.8
4.7
gr/dscf
0.050
0.017
0.024
0.446
0.002
ppm
384
1
A-90
-------
FIELD DATA
I
VD
PLANT REPUBLIC STEEL CLEVELAND, OH
SAMPLING LOCATION NO.l COKE BATTERY
SAMPLE TYPE PART/S02/H2S04
OPERATOR BRUFFEY
AMBIENT TEMP. (DEC. F) 58.
BAR. PRESS. (IN. H6) 29.78
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530087
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .64
THERM. NO.
LEAKAGE .015 CFM 9 4.0 IN.HG
METER CALIB. FACTOR 1.044
READ t RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INlt
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
60.0
90.0
100.0
110.0
120.0
TIME
(24-HR
PI flf* tf \
ILUCK J
956 ~
1008
1016
1028
1038
1046
1056
1106
1116
1126
1138
1148
1156
READING
(CU.FT.)
15.19*
20.070
24.910
29.510
34.130
36.750
43.360
47.960
52.600
56.870
61.510
66.180
70.795
HEAD
(IN.H2U)
.065
.065
.060
.060
.060
.060
.060
.060
.050
.060
.060
~ .060
DIFFERENTIAL
(IN.
DES1RCU
.80
.80
.73
.73
.73
.73
.73
.73
.61
.73
.73
.73
H20)
ACTUAL
.60
.80
.73
.73
.73
.73
.73
.73
.61
.73
.73
.73
STACK
TEPP
(DEG.F)
567.
519.
S31.
539.
536.
552.
564.
520.
529.
542.
533.
552.
DATE 10/28/81
HUN NUMBER 3-2
PROBE LENGTH & TYPE a* HEATED GLASS
KUZZLE : l.D. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER 0
PETER BOX NUMBER FIO
PETER HEAD DIFF. 1.80
C FACTOR .06
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .15
DKY GAS METER PUPP SAPPLE IPPINGER
TEMP
(DEG
INLET
57.
58.
61.
63.
6
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND* OH BRUFFEY
TEST
3-2
NO.l COKE BATTERY
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
V
ON
CP
PM
1 VM
VD
TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
10/28/81
958
1158
120.
12
1.
.
.
•
55.
62.
58.
0
044
397 IN
84
73 IN-H20
603 CU-FT
0 F
547 SCF
METRIC UNITS
10/28/81
958
1158
120
12
1
10
18
1
16
1
.0
.044
.1
.84
.6
.574
.7
.658
MM
PM-H2U
CU-M
C
SCM
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL.ML,
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
§Nd PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.» DRV
P02 PERCENT 02 BY VOX., DRV
PCO PERCENT CO BY VOL.* DRY
PN2 PERCENT N2 BY VOL.* DRY
Mb MOLECULAR NT-DRY STACK GAS
MNS MOLECULAR NT-STACK GAS
ff4.0
7.249 SCF
154.0
.205 SC*
11.02
.890
2.30
10.90
.00
86.80
28.80
27.61
11.02
.890
2.30
10.90
-.00
86.80
28.80
27.61
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
033TO STACK FLOW RATE* DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 OES F, 29.92 IN.H6.
29.78 IN-HG
-1.20 IN-H20
29.69 IN-HG
540. F
19.4 FPS
7466. 30-IN
1689593. SCFH
3635039. ACFH
104.9
.0
.0000 GR/DSCF*
.000 LB/HR
756.41 KM-HG
-30.48 KM-M20
754.17 CM-MG
eez. c
5.9 KP8
4.817 SO-M
47844. SCMH
102650. *CMH
104.5
.0
.000 CG/OSCK
.00 KG/HH
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 3-?
NO.l COKE BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO * (17.647 • VM * Y • (PB * PM / 13.6)) / (TM * 460.)
17.647 * 55.603 * 1.044 * ( 29.78 * .732 / 13.6)
VMSTO « ........ . = 58.517 DSCF
( 62. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC » .04707 • VLC
VWC • .04707 •' 154. « 7.25~SCF
PERCENT MOISTURE IN STACK GAS
BMO • (100. • VNC)*/ (VMSTD * VWC)
IP 100. • 7.25
I BHO * —— .— > 11.02 PERCENT
vo 58.547 » 7.25
>e»
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - BNO) / 100.
100. • 11.0
FMD « —.-————.—— s .890
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MD » (PC02 * .44) » (P02 * .32) t (PN2 » PCO) * .28
MO > ( 2.30*44/100) «• (10.9*32/100) » ((86.8* .0) * 28/100 s 28.80
MOLECULAR HEIGHT OF STACK GAS
MHS * MO • (1. • (BNO/100)) * 18. * (BNO/100)
MMS = 28.80* (1. -(11.02/100)) * 18. • (11.02/100) s 27.61
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OtLP « SUM. OF THE SORUVH • ITS * 460.))
VS * 85.49 * CP * OELP / (SORT(MMS * PS) * PNTS)
VS * 05.49 * .84 * 92.927 / (30RT( 27.61 * 29.69) * 12. = 19.42 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS » 19.42 * 7466. 3600/144 * 3625039. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD « 17.647 • OS * PS * (17 - (B»»0/10~0)) / (TS * 460.)
17.647 * 3625039. * 29.69 * (1. • (11.02/100))
OSSTD » —————————— —......................... T 1689592. SCFH
( 540. * 460.)
PERCENT ISOKINETIC
I ISO • (30S.5B*(TS«460.))*((0.002669*VLC)«(VM*V*(PB*(PM/13.6))/(TM«460.)))/(TT*VS*PS*ON*ON)
VD
01 (305.58M 540;+460.))*((0.0026697 154.)*( 55.603*1.OOd* ( 29.78*( .732/13.6))/( 62.+460.)))
ISO « —.———.—— .......... .. ..... . . . * 104.51 PEKCtM
120. • 19.42 • 29.69 • .397 * .397
PAftTtCULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 • MN • 15.43 / VMSTO
CS * 0.001 * .0 • 15.43 / 58.547 * .000 GR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR * CS • OSSTD / (15.43 * 453.6)
PMR « .000 • 1689592. V (15.43 • 453.6) • .00
-------
Run No. 3.2
o
Sample volume = 1.66m .58.55 scf
Example calculations
CS (Part) =156.9/1.66= 94.5 mq/m3
CS (Part) = 0.001 x!56.9x 15.43/58.55= 0.041 qr/dscf
CS (S02) =1540/1.66=927.7 ma/m3
= 927.7 x 24.06/_64_ = 349 ppm
= 0.001 x1540 x 15.43/58.55 = 0.406 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2$04
As H2S04.2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
156.9
34.2
0.0
0.0
1540
8.6
2 Concentration,
mg/m
94.5
20.6
0.0
0.0
927.7
5.2
gr/dscf
0.041
0.009
0.000
0.000
0.406
0.002
ppm
349
1
A-96
-------
FIELD OAT»
I
V£>
-J
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TTPE 3-3-M8-350
OPERATOR CLARKE
AMBIENT TEMP. (DEG.F) 58.
BAR. PRESS. (IN. H6) 29.78
STATIC PRESS. UN. HZO) -1.20
FILTER NUMBER(S) 3530080
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 2.0 IN.HG
METER CALIB. FACTOR .992
READ ft RECORD DATA EVERT 10.0
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
00.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
ft nf v I
CLUCKJ
955
1005
1015
1025
1035
1045
1055
1105
1115
1125
1135
1145
ilSS
GAS METER
READING
(CU.FT.)
525.179
530.233
535.270
539.087
544.864
549.778
554.615
559.325
564.660
568.622
573.180
578.160
583.158
MINUTES
VELOCITY
HEAD
(IN.H20)
.065
.060
.060
.070
.060
.060
.060
.060
.050
.060
.060
.060
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESlKfcU
.79
.74
.74
.87
.74
.74
.74
.74
.60
.74
.74
.74
H20)
ACTUAL
.79
.74
.74
.87
.74
.74
.74
.74
.60
.74
.74
.74
STACK
TEKP
(DEG.F)
546.
514.
525.
537.
550.
548.
558.
517.
528.
537.
527.
545.
DATE 10/28/81
RUN NUMBER 3-3
PROBE LENGTH ft TYPE 4* GLASS HEATED
NUZZLE : I.U. .394
ASSUMED KOISTUWE 12.0
SAMPLE BOX NUPBER
PETEH BOX NUMBER FBI
MEIER HEAD OIFF. i.e7
C FACTOR .88
HHOBE HEATER SETTING 350.
HEATER BUX SETTING 350.
HEFEHENCt PBfcSS. DIFF. .15
DKY GAS METER
TtMP
(DEG.F)
INLtT UUTLtT
60. 55.
62. 5b.
66. 56.
69. 50.
71. 58.
72. 58.
74. 60.
76. 60.
77. 62.
76. 62.
76. 63.
76. 62.
PU»»P
VACUUM
(IN.HG)
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
SAMPLE
BOX TEMP
(DEG.F)
394.
378.
335.
327.
300.
352.
354.
354.
350.
349.
352.
346.
IMPINGER
TEMP
(DEG.F)
48.
46.
48.
48.
50.
52.
52.
50.
52.
54.
55.
50.
TOTALS
AVERAGE
120.0
57.979
.74
,74 536.
71.
59.
2.0 353.
50.
-------
PARTICULATE FIELD DATA S RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
3-3
COKE OVEN OUTLET
TEST DATE
I
VD
00
TB TIME-START
TF TIME-FINISH
TT NET TIME OF TESTt MIN.
NP NET SAMPLING POINTS
T METER CALIBRATION FACTOR
ON SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRT GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTO VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL HZO COLLECTED IN
IMPINGERS AND SILICA GEL. ML.
VNC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
•MO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL.. DRY
PN2 PERCENT N2 BY VOL.r DRY
MO MOLECULAR MT-DRY STACK GAS
MMS MOLECULAR MT-STACK GAS
ENGLISH UNITS
10/28/81
1155
120.0
12
.992
,39a IN
.84
.74 IN-H20
57.979 CU-FT
65.2 F
57.660 SCF
218.3
10.275 SCF
"15.13
.649
2.30
10.90
.00
86.60
28.60
27.17
METRIC UNITS
10/20/61
955
1155
120.0
12
.992
10.0
.84
18.9
1.642
18.4
1.633
216.3
.291
15.13
.809
2.30
10.90
.00
86.80
26.80
27.17
MM
MM-H20
CU-M
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
QSSTO STACK FLOH RATE* DRY*
OS ACTUAL STACK FLOM RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEG Ff 29.92 IN.HG.
29.76 IN-HG
•1.20 IN-H20
29.69 IN-HG
536. F
19.6 FPS
7066. 30-IN
1633571. SCFH
3656571. ACFH
106.1
.0
.0000 GR/OSCF*
.000 LB/HR
.01 KM-HG
-30.46 MM-H20
750.17 fM-HG
280. C
6.0 PPS
0.817 SO-M
06258. SOH
103600. »CMH
108.1
.0
.000 PG/DSCK
.00 KG/HH
I
VD
VD
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 3-3
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.647 • VM • Y • tPB » PM / 11.6)) / (TM 4 460.)
17.647 * 57.979 * .992 * ( 29.78 * .743 / 13.6)
VMSTO * ———————————— --- ...... — ..... — - 57.660 DSCF
( 65. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VHC « .04707 * VLC
VHC « .04707 • 218. « 10728 StF
PERCENT MOISTURE IN STACK GAS
BHO • (100. • VMCJ f (VMSTD *
> 100. • 10.28
1 BHO * —————— z 15.13 PERCENT
57.660 * 10.28
MOLE FRACTION OF DRY STACK GAS
FMD • (100. - BHO) / 100.
100. - 15.1
FMD • —————— s .849
100.
AVERAGE MOLECULAR HEIGHT OP DRY STACK GAS
MO s (PC02 • .44) * (P02 * .32) * (PN2 * PCO) * .28
MD * ( 2.30*44/100) * (10.9*32/100) » ((86.8* .0) * 28/100 = 28.80
MOLECULAR HEIGHT OF STACK GAS
MHS s MD * (1. - (BHO/100)) * 18. * (BHO/100)
MHS * 28.80* (1. •(15.13/100)) + 18. • (15.13/100) * 27.17
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE SQRTtVH * (TS * 460.))
VS • 05.49 • CP * OELP / (SORT(MRS * PS) * PNTS)
VS * 65.49 * .84 * 93.030 / (SORT( 27.17 • 29.69) * 12. = 19.60 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS * VS * AS • 3600/144
OS * 19.60 • 7466. 3600/144 * 3658571. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD » 17.647 * OS • PS • (1. • (BMO/100)) / (TS * 460.)
17.647 * 3658571. * 29.69 • (1. - (15.13/100))
OSSTD » ———————————————— — — — = 1633571. SCFH
( 536. » 460.)
> PERCENT I30KINETIC
I
|-J ISO » (305.58*(TS»460.))«((0.002669«VLC)*(VMoY*(PBt(PH/13.6))/(TM*460.)))/(TT*VS*PS«DN*DN)
o ...
1-1 (305.58V( 556.*460.))«(tO.002669* Zi8.)*( 57.97<*« .992*t 29.78*1 .743/13.6))/( 6S.*460.)))
ISO « ———————————————--—-—..——— — -—— — --—— — — - ———-«---•-•• * 108.09 PERCENT
120. * 19.60 • 29.69 * .394 * .394
PARTICIPATE LOADING -- EPA METHOD 5 (At STANDARD CONDITIONS)
CS * 0.001 * MN • 15.43 / VMSTD
CS * 0.001 * .0 * 15.43 / 57.660 * .000 GR/DSCF
PARTICIPATE LBS/HR — EPA METHOD 5
PMR a CS * OSSTO / (15.43 • 453.6)
PMR « .000 • 16J3571. / (15.43 * 453.6) = .00
-------
Run No. 3.3
o
Sample volume = 1.63 m . 57.66 scf
Example calculations
CS (Part) =87.3 /1.63= 53.6 ma/m3
CS (Part) = 0.001 x87.3 x 15.43/ 57.66= 0.023 qr/dscf
CS (S02) =1680/1.63=1030.6mg/m3
=1030.6X 24.06/64 = 387 ppm
= 0.001 x1680 x 15.43/57.66 = 0.450 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
87.3
25.3
34.6
1680
67.2
2 Concentration,
mg/m
53.6
15.5
21.2
1030.7
41.2
gr/dscf
0.023
0.007
0.009
0.450
0.018
ppm
387
10
A-102
-------
FIELD DAT*
O
U)
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 3-4-M8-350
OPERATOR CLARKE
AMBIENT TEMP.(OEG.F) 58.
BAR. PRESS. (IN. HG) 29.78
STATIC PRESS. UN. H20) -1.20
FILTER NUMBER(S) 3530046
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM a 2.0 IN.HG
METER CALIB. FACTOR 1.010
READ * RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSUHE
POINT
NO.
INIT
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
SO.O
60.0
70.0
80.0
90.0
100.0
110.0
120.0
TIME
(24-HR
9S8
1008
1018
1028
1038
1048
1058
1108
1118
1128
1138
1148
1158
READING
(CU.FT.)
950.042
954.880
959.555
964.200
968.911
973.615
978.290
982.900
987.697
992.074
996.815
1.270
6.194
HEAD
(IN.H20)
.065
.065
.060
.060
.060
~ .060
.060
.060
.050
.060
.060
.060
DIFFERENTIAL
(IN.
DESIRED
.79
.79
.74
.74
.74
.74
.74
.74
.60
.74
.74
.74
H20)
ACTUAL
.79
.79
.74
.74
.74
.74
.74
.74
.60
.74
.74
.74
STACK
TEMP
(DEG.F)
567.
519.
531.
539.
537.
552.
564.
520.
526.
540.
532.
552.
DATE 10/28/81
HUN NUMBER 3-4
PROBE LENGTH ft TYPE 5 FT GLASS HEA1EO
NOZZLE I 1.0. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER
KETEH BOX NUMBER FB5
METER HEAD OIFF. 1.86
c FACTOR .88
PHOBE HEATER SETTING 350.
HEATER BUX SETTING 350.
REFERENCE PRESS. OIFF. .15
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM
(OEG
INLET
66.
67.
72.
73.
77.
80.
82.
04.
85.
66.
65.
86.
.F) (IN.Hb)
OUTLET
64.
64.
66.
67.
69.
72.
73.
74.
76.
77.
78.
78.
.0
.0
.0
.0
.U
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(DEG.F)
284.
322.
328.
314.
337.
349.
353.
341.
348.
356.
344.
354.
TEMP
(DEG.F)
40.
38.
40.
40.
40.
40.
42.
42.
46.
44.
44.
46.
TOTALS
AVERAGE
120.0
56.152
.74
.74 540,
79,
72,
1.0
336.
42.
-------
PARTICIPATE FIELD DATA A RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADEN
REPUBLIC STEEL CLEVELAND CLARKE
TEST
3-4
COKE OVEN OUTLET
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
> VM
I—1
0 TM
VMSTO
VLC
VNC
BNO
FMD
PC02
P02
PCO
PN2
MO
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL M20 COLLECfEO IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL.^ DRY
PERCENT CO BY VOL.* DRY
PERCENT N2 BY VOL.* DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR MT-STACK GAS
ENGLISH UNITS
10/28/81
938
1158
120.0
12
1.010
.397 IN
._. •8fl
,74 IN-H20
56.152 CU-FT
75.0 F
55.806 SCF
ifri.9
7.621 SCF
12.01
.880
2.30
10.90
.00
86.80
28.80
27.51
METRIC UNITS
10/28/81
9b8
Ilb8
120.0
12
1.010
10.1
.ea
18.7
1.590
23.9
1.580
161.9
.216
12.01
.880
2.30
10.90
.00
86.80
28.80
27.51
KM
MM-H2U
CU-M
C
SCH
SCf
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK CAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK 6AS VELOCITY
AS STACK AREA
OSSTO STACK FLOW RATE* DRY*
OS ACTUAL STACK FLOM RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEG F, 29.92 iN.HG.
29.76 IN-MG
-1.20 IM-H20
29.69 IN-HG
540. F
19.5 FPS
7466. 30-IN
1674132. SCFH
3631694. ACFH
100.5
.0
.0000 GR/OSCF*
.000 LB/HR
756.ai *M-HG
-30.46 HH-H20
754.17 »H-HG
282. C
5.9 »P3
4.617 SO-M
47406. SCf'H
102639. ACCH
100.5
.0
.000 KG/DSC*'
.00 KG/HK
I
\->
o
-------
>
I..
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 3-4
COKE OVEN OUTLET
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.647 • VM • T • IPB * PM / 13.6)) / (TM + 460.)
17.647 * 56.152 • 1.010 * ( 29.78 » .737 / 13.6)
VMSTD « ————————— --- ....... ------------------ - 55.B06 OSCF
( 75. * 460.)
VOLUME OF WATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 • VLC
VHC • ".04707 * i62. « 7.62 SCF
PERCENT MOISTURE IN STACK GAS
BHO « (100. «~ VWCi /"(VMSTO «~V»»C) ~~~
100. * 7.62
BMO * ——————— * 12.01 PERCENT
55.806 * 7.62
o
^ MOLE FRACTION OF DRT STACK GAS
FMD » (100. - BHO) / 100.
100. - 12.0
FMD « ————— * .esc
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK 6(51
MD * (PC02 * .44) + (P02 • .32) + (PN2 * PCO) * .28
MD * ( 2.30*44/100) • (10.9*32/100) * ((86.6* .0) • 28/100 = 28.60
MOLECULAR HEIGHT OF STACK GAS
MMS » MD * (1. - (BNO/100)) * 18. * (BNO/100)
MMS » 28.80* (1. -(12.01/100)) » 18. * (12.01/100) s 27.51
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP » SUM. OF THE SQRT(VH * (TS * 460.if
VS « 65.49 • CP • OELP / (SORT(MMS • PS) * PNTS)
VS • 85.49 * .84 * 92.915 / (SORT( 27.51 * 29.69) • 12. = 19.46 FPS
STACK 6A8 VOLUMETRIC FLO* AT STACK CONDITIONS
OS • VS * AS * 3600/144
OS * 19.46 * 7466. 3600/144 • 3631694. ACFH
STACK GAS VOLUMETRIC FLOM AT STANDARD CONDITIONS
OSSTD « 17.64? • OS • PS * (1. • (BMO/106)) / (TS * 460.)
17.647 • 3631694. * 29.69 * (1. • (12.01/100))
OSSTO • ——« ..... .... ... r 167«13*. SCFM
( 540. * 460.)
PERCENT ISOKINETIC
. ISO * (305.58*(TS*460.))*((0.002669*VLC)*(VM*T*(PB*(PM/13.6))/(TM»460.)))/ I TT*V3*PS*DN*DN)
I>
M (305.58*( 540.M60.))*((0.002669* 162.)*( 56.152*1.010*( 29.78»( .737/13.6))/( 75.4460.)))
O ISO » ———-—..-.—.——.—...——.—.———............................................... c 100.54 PERCENT
"^ 120. • 19.46 * 29.69 • .397 * .397
PARTtCULATE LOADING"-- EPA METHOD 5 UT'STANOARD CONDITIONS)
CS « 0.001 * MN • 15.43 / VMSTD
CS • 0.001 * .0 * 15.43 / 55.806 * .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR B CS * OSSTD / (15.43 « 453.6)
PMR * .000 • 1674132. / (15.43 * 453.6) = .00
-------
Run No. 3.4
o
Sample volume = 1.58m t 55.81 scf
Example calculations
CS (Part) =40.3 /1.58= 25.5 mq/m3
CS (Part) = 0.001 x40.3 x 15.43/65.81 =0.011 qr/dscf
CS (S02) =1620/1.58= 1025ma/m3
= 1025 x 24.06/64 =385 ppm
= 0.001 x1620 x 15.43/55.81 =0.448 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2$04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
40.3
3,7
5.0
1620
89.2
3 Concentration,
mg/m
25.5
2.3
3.2
1025.3
56.4
gr/dscf
0.011
0.001
0.001
0.448
0.025
ppm
385
14
A-108
-------
FIELD DATA
I
M
O
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE STACK
SAMPLE TYPE METHOD 5-250
OPERATOR 00/MP
AMBIENT TEMP.(DEG.F) 55.
BAR. PRESS. (IN. H6) 29.78
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530058
STACK INSIDE DIM. (IN) 47.50 .00
PITOT TUBE COEFF. .ea
THERM. NO.
LEAKAGE .012 CFM 9 9.
METER CALIB. FACTOR 1.033
READ * RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT TIME
NO. (MIN.
INIT 0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.6
TOTALS 120.0
TIME
) (24-HR
<*• nr*H i
LLUCKI
947
957
1007
1017
1027
1037
~1047
1057
1107
1117
1127
1137
~ U4f
READING
(CU.FT.)
719.921
724.750
729.570
734.430
739.300
744.250
749.140
754.100
759.070
764.050
769.030
774.000
7?9.017
59.096
HEAD
(IN.H20)
.075
.075
.075
.075
.075
~,075
.075
.075
.075
.075
.075
~.0?S
CLEVELAND
3 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.77
.77
.77
.77
.77
~ .77
.77
.77
.77
.77
.77
.77
H20)
ACTUAL
.77
.77
.77
.77
.77
.77
.77
.77
.77
.77
.77
.77
STACK
TEKP
(OEG.F)
518.
518.
518.
518.
518.
518.
518.
518.
518.
518.
518.
518.
DATE 10/28/81
HUN NUMBER 3-5
PROBE LENGTH S TYPE 6* GLASS
NUZZLE 6-1051 I.D. .374
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
PETER BOX NUMBER FB4
PETER HMD D1FF. 1.88
C FACTOR .92
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .is
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP
(DEG
INLET
60.
61.
61.
69.
M.
73.
75.
76.
75.
75.
75.
75.
.F)
OUTLET
59.
59.
60.
62.
63.
65.
67.
68.
66.
69.
69.
69.
VACUUM
(IN.HG)
7.4
7.7
7.9
8.1
8.2
.5
.7
.8
.8
.8
.8
.9
BOX TEMP
(OEG.F)
226.
230.
234.
241.
227.
228.
225.
226.
228.
225.
230.
227.
TEMP
(DEG.F)
36.
36.
38.
36.
38.
38.
40.
40.
00.
38.
40.
40.
AVERAGE
.77
.77 518.
71.
65.
6.4 229.
39,
-------
I-
\->
o
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST fEAM LEADER
REPUBLIC STEEL CLEVELAND DO/HP
TEST
3-5
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
VM
TM
VMSTO
VLC
VHC
BNO
FMD
PC02
P02
PCO
PN2
MD
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H26 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL.. DRY
PERCENT 02 BY VOL. V OR V
PERCENT CO BY VOL.* DRY
PERCENT N2 BY VOL.* DRY
MOLECULAR MT-ORY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/28/81
947
1147
120.0
12
1.033
.374 IN
.64
.77 IN-H20
59.096 CU-FT
67.8 f
60.900 SCF
189.7
8.506 SCF
T2.25
.877
2.30
HJi90
.00
86.80
28.60
27.48
METRIC UNITS
10/28/81
947
1147
1?0.0
12
1.033
9.5
.64
19.6
1.673
19.9
1.724
180.7
.241
12.25
.877
2.30
10.90
.00
86.80
28.80
27.48
CM
KM-H20
CU-M
C
sew
SCK
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
T8 AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLON RATE, DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5 _
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 OE6i'F» 29,92 IN.H6.
29.78 IN-HG
-1.20 IN-M20
29.69 IN-HG
518. F
21.5 FPS
30-IN
SCFH
ACFH
7466.
1889290.
4018903.
109.5
.0
.0000 GR/OSCF*
.000 LB/HH
756.ai MH-MG
-30.48 MM-H20
750.17 KM-HG
270. C
6.6 I" PS
4.817 30-M
53499. 3CWH
113803. *C*M
109.5
.0
.000 NG/DSO
.00 KG/HR
>
I
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 3-5
COKE STACK
VOLUME OF DRY 6A3 SAMPLED AT STANDARD CONDITIONS
VMSTO* (17.647 • VW •" Y • IPB * PM / 13~.6>) / (TM » 060.)
17.647 • 59.096 * 1.033 • ( 29.78 * .770 / 13.6)
VMSTD * ——————— — —..................... = 60.900 D3CF
( 60. » 460.)
VOLUME OF WATER VAPOR AT STANDARD CONDITIONS
VMC » .04707 * VLC
VNC « .04707 • 181. » ~ 8.51 SCF
PERCENT MOISTURE IN STACK GAS
BNO » (100. • VHCl / (VMSTD * VHC)
100. * a.si
BNO « —————————— * 12.25 PERCENT
60.900 * 8.51
,. . .... . .„
MOLE FRACTION OF DRY STACK GAS
FMD » (100. - BMO) / 100.
100. - 12.I
FMD * ————— c .877
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK Stf
MD * (PC02 * .44) * (P02 * .32) + (PN2 * PCD) * .28
MD * ( 2.30*44/100) • (10.9*32/100) * ((86.8* .0) * 28/100 * 28.80
MOLECULAR HEIGHT OF STACK GAS
MNS * MD • (1. • (BMO/100)) + 18. * (BHO/100)
MHS a 28.80* (1. -(12.25/100)) * 18. * (12.25/100) « 27.48
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SQRTIVM • ITS * 460.))
VS a 65.49 • CP • OELP / (SORT(MHS • PS) * PNTS)
VS s 85.49 * .84 • 102.770 / (SORTl 27.48 » 29.69) * 12. = 21.53 FPS
STACK GAS VOLUMETRIC FLO" AT STACK CONDITIONS
OS z VS * AS * 3600/144
OS 3 21.53 • 7466. 3600/144 a 4018903. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO • IT.647 • OS • PS * (1. - (BMO/lOO)) / (TS * 460.)
17.647 * 4018903. • 29.69 * (1. - (12.25/100))
OSSTD « ————————..———.— —— = 1689290. SCFH
( 518. * 460.)
PERCENT ISOKINETIC
> ISO a (305.58*(TS»460.))*((0.002669*VLCmVM*Y*(PB«(PM/13.6))/{TM»460.)))/(TT*VS*PS*DN*DN)
I
I-1 (30b.58*( SlB.+460.))*((6.002669* ~ iel.)*( 59.096*1.033*( 29.78*1 .770/13.6))/( 68.+460.)))
f"J ISO « —————— — .. .... . — • 109.54 PERCENT
120. • 21.53 * 29.69 * .374 * .374
PARTICIPATE LOADING— EPA METHOD 5 (AT STANDARD CONDITIONS)
CS a 0.001 * MN * 15.43 / VMSTD
C3 a 0.001 • .0 * 15.43 / 60.900 a .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR a CS * OSSTD / (15.43 * 453.6)
PMR « .000 * "1889290. / (15.43 * 455.6) s .00
-------
Run No. 3-5
Sample volume = 1.72 m3. 60.90 Scf
Example calculations
CS (Part) =171.2/1.72= 99.5 mq/m3
CS (Part) = 0.001 x171.2 x 15.43/60.90=0.043 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
171.2
29.0
26.8
26.2
25.2
22.0
0.0
0.0
99.1
3.2
77.3
- Concentration,
mg/m
99.5
16.9
15.6
15.2
14.6
12.8
0.0
0.0
57.6
1.9
44.9
gr/dscf
0.043
0.007
0.007
0.007
0.006
0.006
0.0
0.0
1
0.025
0.001
0.020
ppm
A-114
-------
FIELD DATA
Cn
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE STACK
SAMPLE TYPE METHOD 8-600
OPERATOR DO/HP
AMBIENT TEMP.(DEG.F) 55.
BAR. PRESS. (IN. HG) 39.78
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530025
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 12.0 IN.HG
METER CALIB. FACTOR .962
READ > RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE STACK
POINT TIME TIME READING HEAD DIFFERENTIAL T£f»P
NO. (MIN.) (24-HR (CU.FT.) (IN.H20) (IN.H2U) (DEG.F)
INif 0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
SO.O
90.0
100.0
110. 0
120.0
vuuvn f
950
1000
1010
1020
1030
1040
1050
1100
1110
1120
1130
1140
1150
DESIRED ACTUAL
203.451
208.690
214.260
219.700
225.150
230.620
236.040
241.550
247.000
252.490
257.960
263.460
266.908
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
4.72
4.72
4.72
4.72
.72
.72
.72
.72
.72
.72
.72
.72
.00
.00
.00
.00
.00
.00
.00
.00
.00
.00
.00
.00
518.
518.
516.
516.
516.
518.
518.
518.
518.
518.
516.
516.
DATE 10/26/81
HUN NUMBER 3-6
PHOBE LENGTH S TYRE 4* OUAHTZ
NUZZLE : I.U. .590
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
PETER BOX NUMBER FB8
PETER HtAD OIFF. 1.91
C FACTOk .94
PROBE HEATEH SETTING 600.
HEATER BOX SETTING 600.
REFERENCE PRESS. OIFF. .03
DHY GAS METER PUPP SAMPLE IMPINbEK
TEMP VACUUM BOX TEMP TEMP
(DEG.F) (IN.HG) IDEG.F) (OEG.F)
INLET OUTLET
54.
56.
60.
64.
66.
68.
69.
69.
69.
69.
70.
70.
52.
52.
53.
54.
55.
57.
56.
59.
59.
6U.
61.
61.
4.0
4.0
4.2
4.2
4.3
6.2
6.6
9.3
9.3
9.4
9.6
11.2
577.
556.
553.
526.
580.
538.
565.
574.
576.
565.
566.
537.
34.
3«.
36.
40.
38.
34.
38.
40.
40.
40.
42.
42.
TOTALS
AVERAGE
120.0
65.457
4.72
1.00
518.
65,
57.
7.0
560.
38.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO/MP
TEST
3-6
COKE STACK
TEST 0
TB
TF
TT
NP
V
ON
CP
PM
ATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
ENGLISH UNITS METRIC UNITS
10/28/81 10/28/61
950 950
1150 1150
120.0 120.0
12 12
.982 .982
.590 IN 15.0 **
•8fl •»
-------
PB BAROMETRIC PRESSURE
P9I STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
T3 AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE, DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 OE6 F, 29.92 iN.HG.
29.78 1N-HG
-1.20 IN-M20
29.69 IN-HG
518. F
21.8 FPS
7466. SQ-IN
1790817. SCFH
4063123.
49.6
.0
ACFH
.0000 GR/OSCF*
.000 LB/HR
756.41 VM-HG
-30.18 *M-M2U
754.17 KM-HG
270. C
6.6 VPS
4.817 SO-M
50694. SCKH
115055. ACMH
49.6
.0
.000 PG/DSCf
.00 KG/HH
>
I
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 3-6
COKE STACK
VOLUME OF ORT GAS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 • VM * V * (PB * PM / 13.6)) / (TM * 460.)
17.647 * 65.457 • .902 • ( 29.78 » 1.000 / 13.6)
VMSTD • ———————————............—........... - 64.S92 OSCF
( 61. » 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VNC » .04707 • VLC
VNC * .04707 * 29$. * 14.04 SCF
PERCENT MOISTURE IN STACK GAS
BHO * (100. * VMC) / (VMSTD * VHC) ~'~
> ...
' 100. * 14.04
\L BMO « —.——.....—......... a 17.76 PERCENT
00 64.992 * 14.04
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - 8NO) / 100.
100. -~ 17.8
FMD « ————.———. * .822
100.
AVERAGE MOLECULAR WEIGHT of DRY STACK GAS
MO * (PC02 • .44) * (P02 • .32) * (PN2 * PCO) • .28
MO * ( 2.30*44/100) * (10.9*32/100) * 1(86.8* .0) * 28/100 = 28.80
MOLECULAR HEIGHT OF STACK GAS
MNS * MO » (1. - (BNO/100)) * 18. * (BWO/100)
MNS * 28.80* (1. -(17.76/100)) + 16. • (17.76/100) * 26.89
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP » SUM. OF THE SORTCVH * ITS * 060.))
VS * 85.09 • CP • OELP / (SORT(MRS • PS) * PNTS)
VS * 85.49 • .84 • 102.770 / (SORT( 26.89 • 29.69) * 12. = 21.77 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS • AS * 3600/144
OS • 21.77 * 7466. 3600/144 • 4063123. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTD • 17.607 • OS • PS * (1. • (BMO/10~6)) / (TS » 460.)
17.647 * 4063123. * 29.69 • (1. - (17.76/100))
OSSTO « — ——~ —— — s 1790217. SCFH
( 518. » 060.)
PERCENT ISOKINETIC
jL ISO « (305.58MTS»460.))«((0.002669«VLC)*(VM«Y*(PB*(PM/13.6))/(TM««60.)))/(TT*VS«PS«DN«DN)
M
^ (305.58*( S18.+460.))*((0.002669* Z98.)«( 65.057* .982*( 29.78»( 1.000/13.6))/( 61,»060.)))
ISO • —.—.—————————————.—— — — —————— ———— — — — — — 8 49.58 PERCENT
120. • 21.77 • 29.69 * .590 * .590
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
CS > 0.001 * .0 • 15.43 / 64.992 « .000 GR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR « CS • QSSTD / (15.43 • 453.6)
PMR 8 .000 * 1790217. / (15.43 * 453.6) * .00
-------
Run No. 3.6
Q
Sample volume =1.84 m r 64.99 scf
Example calculations
CS (Part) =36.0/1.84=19.6 mq/m3
CS (Part) = 0.001 x36.0 x 15.43/64.99= 0.008 qr/dscf
CS (S02) =1720/1.84=935 mg/m3
= 935 x 24.06/64 =351 ppm
= 0.001 x!720 x 15.43/64.99 =0.408 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
36.0
4.2
5.7
1720
164
., Concentration,
mg/m
19.6
2.3
3.1
935
89.1
gr/dscf
0.008
0.001
0.001
0.408
0.039
ppm
351
22
A-120
-------
FIELD DATA
>
I-1
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
REPUBLIC STEEL CLEVELAND
NO.l COKE BATTERY OUTLET
PART/H2S04/S02
BHUFFEY
AMBIENT TEMP.(OEG.F) 56.
BAR. PRESS. (IN. H6) 39.81
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530039
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .64
THERM. NO.
LEAKAGE .Ota CFM 9 17.
METER CALIB. FACTOR 1.003
READ « RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT
NO.
INlf
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
62.0
TIME
(24-HR
* f*l Of* tf %
CLUCKJ
1540
1550
1600
1610
1620
1630
1704
1716
READING
ICU.FT.)
638.776
643.860
646.930
654.010
659.090
664.160
669.540
673.150
HEAD
(IN.H20)
.060
.060
.060
.060
.060
.070
.030
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
UESIREU
.73
.73
.73
.73
.73
.87
.37
H20)
ACTUAL
.73
.73
.73
.73
.73
.87
.37
STACK
TEPP
(DtG.F)
543.
556.
515.
519.
529.
514.
511.
DATE 10/28/81
NUN NUMBER 4-1
PROBE LENGTH S TYPE 5* HEATED GLASS
MUZZLE : I.D. .397
ASSUMED MOISTUKE 12.0
SAKPLE BOX NUMBER 01
PETER BOX NUMBER FB2
PETER MEAD UIFF. 1.76
C FACTOR .86
PROBE HEATER SETTING 250.
HEATER BUX SETTING 250.
REFERENCE PRESS. DIFF. .15
DRY GAS METER PUMP SAMPLE IPPINGEK
TEMP
(DEC
If^LEf
60.
62.
65.
66.
66.
b6.
64.
.F)
OUTLET
60.
6V.
61.
60.
60.
61.
60.
VACUUM
(IN.HG)
2.0
2.0
2.0
4.0
3.0
3.0
8.0
BOX TEMP
(DEG.F)
255.
264.
252.
261.
241.
255.
246.
TEMP
(DEG.F)
47.
48.
4«.
42.
46.
47.
0.
TOTALS
AVERAGE
62.0
34.374
,70
.70 527,
64.
60.
3.4 254.
39.
-------
PARTICIPATE FIELD DATA a RESULTS TABULATION
PLANT" NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
4-1
NO.I COKE BATTERY OUTLET
to
ENGLISH UNITS
TEST
TB
TF
TT
NP
V
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
10/28/61
1540
1716
62
7
1
.0
.003
.397 IN
.84
.70 IN-H20
METRIC UNITS
10/28/81
1540
1716
62
7
1
10
17
.0
.003
.1
.84
.7
KM
MM-
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H26 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VNC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BHO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRV
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR HT-DHY STACK GAS
MHS MOLECULAR MT-STACK GAS
34.374 CU-FT
.973 CU-M
62.4 F
34.761 SCF
IM.I
5.641 SCF
14.38
.656
4.10
11.00
.00
84.90
29.10
27.50
16
124
14
4
11
84
29
27
.9 C
.985 SCM
.1
.165 SCC
.38
.856
.10
.00
.00
.90
.10
.50
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERA6E STACK TEMP
V3 AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLON RATEr ORT*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 29.92 IN.HG.
89.81 1N-HG
-1.80 IN-HZO
29.72 IN-HG
527. F
18.7 FPS
7466. SO-IN
1592300. SCFH
3098600.
127.5
.0
ACFM
.0000 GR/D8CF*
.000 LB/HR
757.17 *M-HG
-30.08 VM-M20
750.93 *M-HG
275. C
5.7 KP3
0.817 SO-M
05089. SCKH
99070. ACMH
187.5
.0
.000 PG/OSCI"
.00 KG/HR
to
u>
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 4-1
NO.l COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 * VM * Y * (PB * PM / 13.6)) / (TM * 460.)
17.647 • 34.374 • 1.003 * ( 29.81 «• .699 / 13.6)
VMSTD » —————— — ————— ............ i 31.781 DSCF
( 62. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 * VLC
VMC • .04707 • 124. a 5.84 SCF
PERCENT MOISTURE IN STACK GAS
BMO » (100. * VMC) / (VMSTD + VMC)
100. * 5.84
> BMO « —.—— ....... s 14.38 PERCENT
^ 34.781 «• 5.84
MOLE FRACTION OF DRY STACK GAS
FMD • (100. • BMO) / 100.
100. - 14.4
FMD « —————— s .856
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD * (PC02 * .44) * (P02 * .32) * (PN2 * PCO) • .28
MO » ( 4.10*44/100) * (11.0*32/100) * ((84.9* .0) * 20/100 = 29.10
MOLECULAR HEIGHT OF STACK GAS
MMS s MD * (1. - (8MO/100)) * 18. * (BMO/100)
MMS » 29.10* (1. -(14.38/100)) + 18. * (14.38/100) « 27.50
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP * SUM. OF THE SORT(VH • (TS * 460.))
VS = 85.49 * CP • OELP / (SORT(M*S • PS) * PNTS)
VS = 85.09 * .84 • 52.236 / (SORT( 27.50 * 29.72) * 7. = 18.74 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS « VS * AS * 3600/144
OS * 18.74 * 7466. 3600/144 • 3498604. ACFH
STACK GAS VOLUMETRIC FLOM AT STANDARD CONDITIONS
OSSTD • 17.647 * OS * PS * (1. - (BNO/IOO)) / (tS » 460.)
17.647 • 3498604. * 29.72 * (1. » (14.38/100))
OSSTD • ————————. ——————- — — ---- x 1592304. SCFH
I 527. * 460.)
> PERCENT ISOKINETIC
£ ISO » (305.58*(TS»460.))»((0.002669«VLC)*(VM«YMPB+(PM/13.6))/(TM*460.)))/(TT*VS«P9*DN*DN)
Ui
(305.58M 527.+460.))*((0.002669* 124.)»( 34.374*1.003*( 29.81*1 .699/13.6))/{ 62.*460.)))
130 a — ........... .. ...... ..... ... ..... . s 127.bl PERCENT
62. * 18.74 * 29.72 • .397 * .397
PARTICIPATE LOADING— EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
CS = 0.001 * .0 * 15.43 / 34.781 « .000 GR/D3CF
PARTICULATE LBS/HR — EPA METHOD 5
PMR • CS * OSSTD / (15.43 * 453.6)
PMR • .000 * 1592304. / (15.43 * 453.6) s .00
-------
Run No. 4.1
Sample volume = 0.99 m3f34.78 scf
Example calculations
CS (Part) =139.9/0.99 = 141.3 mg/m3
CS (Part) = 0.001 x!39.9 x 15.43/34.78 =0.062 qr/dscf
CS (S02) =1300 70.99 =1313.1ma/m3
=1313.Ix 24.06/64 =493 ppm
= 0.001 x1300 x 15.43/34.78 = 0.577 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
139.9
47.5
64.9
1300
11.5
- Concentration,
mg/m
141.3
47.9
65.6
1313.1
11.6
gr/dscf
0.062
0.021
0.029
0.577
0.005
ppm
494
3
A-126
-------
FIELD DATA
M
ro
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PART/H2304/S02
OPERATOR BRUFFEY
AMBIENT TEMP. (DEG.F) 56.
BAR. PRESS. (IN. HG) 29.81
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530081
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 6.0 IN.HG
METER CALIB. FACTOR 1.04a
READ § RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INIT
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
5S.O
58.0
TIME
(24-HR
i*i nrif %
CLUCK/
1543
1553
1603
1613
1623
1633
1710
1718
READING
ICU.FT.)
71.235
75.900
80.590
85.260
89.970
94.585
99.580
100.865
HEAD
(IN.H20)
.060
.060
.060
.060
.060
.070
.030
DIFFERENTIAL
(IN.
DESIRED
.73
.73
.73
.73
.73
.87
.37
H20)
ACTUAL
.73
.73
.73
.73
.73
.87
.37
STACK
TEMP
(DEG.F)
547.
563.
MS.
520.
530.
523.
516.
DATE 10/28/81
RUN NUMBER 4-2
PHOBE LENGTH « TYPE 4' HEATED GLASS
NOZZLE : 1.0. .397
ASSUMED MOISTURE 12.0
SAMPLE BUX NUMBER Q
PETER BOX NUMBbH F10
METEH HIAD DIFF. i.ao
C FACTOR .86
PROBE HEATER SETTING 250.
HEATER BUX SETTING 250.
REFERENCE PRESS. DIFF. .15
ONY GAS METER PUMP SAMPLE IMPINGER
TEMP
(DEG
IKLET
66.
67.
70.
71.
71.
72.
be.
.F)
OUTLET
66.
66.
66.
66.
66.
66.
67.
VACUUM
(IN.Hb)
2.0
3.0
3.0
3.0
3.0
3.0
1.0
BOX TEMP
(DEG.F)
270.
298.
256.
266.
252.
253.
264.
TEMP
(OEG.F)
50.
51.
50.
50.
49.
50.
47.
TOTALS
AVERAGE
58.0
29.630
,70
.70
531,
69.
66.
2.6 266.
50.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
4-2
NO.l COKE BATTERY OUTLET
00
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
DN
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
10/28/81
1 54 j
me
58
7
1
_.
.0
.004
.397 IN
.64
.70 IN-H20
METRIC UNITS
10/26/81
1543
1718
56
7
1
10
17
.0
.044
.1
.84
.7
CM
MM-1
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTO VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H2CCOLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT COS BY VOL., DRY
P02 PERCENT 02 BY VOL.* DRV
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR MT-DRY STACK GAS
MHS MOLECULAR NT-STACK GAS
29.630 CU-FT
67.7 F
30.690 SCF
103.3
4.662 SCF
.839 CU-M
19.6 C
.875 SCC
103.3
.136
13.60
.664
4.10
11.00
.00
84.90
29.10
27.59
13.60
.664
4.10
11.00
.00
84.90
29.10
27.59
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK 6AS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE* DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 6* DEC F, 29.92 IN.H6.
39.81 IN-HG
•1.20 IN-H20
29.72 IN-HG
531. F
te.e FPS
7466. 30-IN
1601155. SCFH
3499941.
120.4
.0
ACFH
.0000 GR/DSCF*
.000 LB/HR
757.17 PM-HG
-30.46 PM-H20
754.93 t'M-HG
277. C
5.7 KPS
4.817 30-M
45340. SCt'H
99108. »CKH
120.4
.0
.000
.00 KG/HR
H
N>
VO
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 4-2
NO.l COKE BATTERY OUTLET
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.607 « VM • T * (PB * PM / 13.6)) / (TM * 460.)
17.647 • 39.630 * 1.044 * ( 39.81 * .699 / 13.6)
VMSTO « ——————————--- ———-- — - -------- --- r 30.690 OSCF
( 68. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC « .04707 * VLC
VHC * .04707 • 103. a ~4.86~SCF
PERCENT MOISTURE IN STACK GAS
BNO • (100. • VHC) /~ (VMSTD * VHC)
^ 100. * 4.86
I BHO » - ----- — — — ---- ..... ... e 13.60 PERCENT
M 30.890 * 4.86
O
MOLE FRACTION OF DRY STACK GAS
FMD • (100. > BHO) / 100.
100. - 13.6
FMD a —.-.———— --- .. • .864
100.
AVERAGE MOLECULAR HEIGHT OF DRV STACK GAS
MD « (PC02 • .44) * (P02 • .32) * CPN2 » PCD) * .28
MO « ( 4.10*44/100) * (11.0*32/100) * ((80.9* .0) * 28/100 = 29.10
MOLECULAR HEIGHT OF STACK GAS
MRS * MD * (1. > (BRO/100)) + 18. * (RHO/100)
MHS * 29.10* (1. .(13.60/100)) * 18. * (13.60/100) * 27.59
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SORTIVH * (TS » 460.))
VS « BS.49 « CP • OELP / (SORT(MNS • PS) • PNT3)
VS » 85.49 * .84 * 53.338 / (SORT( 27.59 * 29.72) * 7. = 16.75 FP3
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS « VS * AS * 3600/144
OS * 18.75 • 7466. 3600/144 • 3099941. ACFH
STACK 9AS VOLUMETRIC FLOM AT STANDARD CONDITIONS
OSSTO « 17.647 • OS • ?3~* U. - (BNO/100)) / (TS * 460.)
17.647 • 3499941. • 29.72 • (1. • (13.60/100))
OSSTO * —————— .. = 1601155. SCFH
( 531. * 460.)
PERCENT ISOKINETIC
ISO * (305.58*(T3+460.))«((0.002669*VLC)«(VM*V*(PB+(PM/13.6))/(TM+ .000 GR/D3CF
PARTICULATE LBS/HR — EPA METHOD 5
PMR * CS * OSSTD / (15.43 * 453.6)
PMR * .000 • 1601155. / (IS.43 * 453.6) > .00
-------
Run No. 4.2
Sample .volume = n.flR m f 3n.RQ scf
Example calculations
CS (Part) =113.2/0.88 = 128.6 mg/m3
CS (Part) = 0.001 x113.2 x 15.43/30.89 = 0.056 qr/dscf
CS (S02) =1170 /0.88 =1329.5mg/m3
=1329.5X 24.06/64 =500 ppm
= 0.001 x 1170 x 15.43/30.89
= 0.584 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H£S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
113.2
41.7
0.4
0.5
1170
11.9
3 Concentration,
mg/m
128.6
47.4
0.4
0.6
1329.5
13.5
gr/dscf
0.056
0.021
0.0002
0.0002
0.584 |
0.006
ppm
500
3
A-132
-------
FIELD DATA
u>
U)
PLANT REPUBLIC STEEL
CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 4-3-M8-400
OPERATOR CLARKE
AMBIENT TEMP. (DEG.F) 56.
BAR. PRESS. (IN.HG) 29.81
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530024
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 5.
METER CALIB. FACTOR .992
READ * RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT TIME ~ TIME READING HEAD
NO. (MIN.) (24-HR (CU.FT.) (IN.H20)
f 1 rt f* H 1
CLUCK 1
INIT 0 1540 583.448
10.0 1550 588.298 .060
20.0 1600 593.200 .060
30.0 1610 597.855 .060
40.0 1620 602.700 .060
50.0 1630 607.666 .060
55.0 1640 613.075 .070
60.0 1715 616.530 .030
0 IN.HG
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H20)
DESIRED ACTUAL
.74 .74
.74 .74
.74 .74
.74 .74
.74 .74
.82 .82
.37 .37
STACK
TECP
(DEG.F)
542.
558.
514.
519.
529.
499.
512.
DATE 10/28/81
NUN NUMBER 4-3
PROBE LENGTH 8 TYPE 4 FT GLASS HEATED
NUZZLE : I.D. .398
ASSUMED MOISTURE 12.0
SAMPLE BOX NUKbER
PETER BOX NUMBER FBI
PETEH HEAD DIFF. 1.87
C FACTOR .88
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
REFERENCE PRESS. DIFF. 1.50
DKV GAS METER PUMP SAKPLE IMPINGEK
TEMP VACUUM BOX TEMP TEMP
(DEG.F) (IN.HG) (DEG.F) (DEG.F)
INLET OUTLET
61. 58. 2.0 285. 54.
64. 56. 2.0 340. 52.
6«. 56. 2.0 365. 52.
72. 60. 2.0 371. 52.
74. 60. 2.0 366. 52.
76. 62. 3.0 355. 54.
70. 62. 2.0 371. 52.
TOTALS
AVERAGE
60.0
33.082
.70
.70 525.
69.
60.
2.1
350,
53.
-------
PARTICIPATE FIELD DATA A RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
a-3
COKE OVEN OUTLET
TEST
TB
TF
TT
NP
Y
DN
CP
PM
DATE
TIME-STARt
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
ENGLISH UNITS
10/28/81
1540
1715
60.0
7
.992
.398 IN
.84
.70 IN-H20
METRIC UNITS
10/26/81
1540
1715
60. 0
7
.992
10.1
.84
17.7
KM
KM-
DROP
tL VM VOLUME OF DRY GAS SAMPLED
U) AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VMC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRV GAS
PC02 PERCENT C02 BY VOL., DRV
P02 PERCENT 02 BV VOL., DRV
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR NT-DRV STACK GAS
MNS MOLECULAR HT-STACK GAS
33.062 CU-FT
.937 CU-M
64.5 F
32.972 SCF
118.1
5.559 SCF
14.43
.856
4.10
11.00
.00
84.90
29 . 1 0
27.50
18
118
14
4
11
84
29
27
.1 C
.934 SCK
.1
.157 SCM
.43
.856
.10
.00
.00
.90
.10
.50
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
QSSTD STACK FLON RATE, DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 66 DEC F, 29.92 iN.HG.
29.61 1N-HG
•1.20 IN-H20
29.72 IN-HG
525. F
18.7 FPS
7466. SO-IN
1593930. SCFH
3094845.
124.2
.0
ACFH
.0000 GR/DSCF*
.000 LB/HN
757.17 f*-Ht
-30.08 *M-H20
750.93 HH-HG
87«. C
5.7 KPS
a.617 SQ-M
05107. SCMH
98960. ACMH
120.2
.0
.000 MG/DSCI"
.00 KG/HH
Ul
U1
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 4-3
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.64? • VM * T * (PB I * PM / 13.6)) / (TM * 460.)
17.647 • 33.002 * .992 * ( 29.81 * .699 / 13.6)
VMSTO • —————— --------- . -------------------------- = 32.97«! OSCF
I 65. » 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 * VLC
VHC * .04707 • li*. » " S.S6 SCF
PERCENT MOISTURE IN STACK GAS
BHO • (100. • VHC) / (VMSTD » VHC)
100. * 5.56
> BHO s — --- .................. x 14.43 PERCENT
I 32.972 * 5.56
U)
cr>
MOLE FRACTION OF DRY STACK GAS
FMD « (100. • BHO) / 100.
100. - 14.4
FMD • —————— 8 .856
100.
AVERAGE MOLECULAR HEIGHT OF DRV STACK GAS
MO * (PC02 • .44) * (P02 • .32) * (PN2 * PCO) * .28
MO > ( 4.10*44/100) • (11.0*32/100) * ((64.9* .0) * 28/100 = 29.10
MOLECULAR HEIGHT OF STACK GAS
MRS « MD * (1. • (BHO/100)) + 18. * (BMO/100)
MNS « 29.10* (i. -(14.45/100)) * 18. * (14.43/100) * 27.50
-------
STACK 6AS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE SORUVH * (TS * 460.))
VS * 85.49 * CP * DELP / (SORT(MRS * PS) • PNTS)
VS > 65.49 * .84 * 52,170 / (SORT( 27.50 * 29.72) * 7. = 16.72 FPS
STACK 6A9 VOLUMETRIC FLOW AT STACK CONDITIONS
OS * VS • A3 * 3600/144
OS > 18.72 * 7466. 3600/144 * 3494845. ACFH
STACK GAS VOLUMETRIC FLOH AT STANDARD CONDITIONS
03STD » 17.647 * OS * PS * (1. » (BHO/100)) / (TS » 460.)
17.647 • 3494845. * 29.72 • (1. - (14.43/100))
OSSTO » ——————--- ——.——............ .—.. - 1592934. SCFH
( 525. * 460.)
PERCENT ISOKINETIC
> ISO • (305.58MT3«460.))*((0.002669*VLC)«(VM*V*(PB«(PM/13.6))/(TM+460.)))/(TT*VS«PS*ON*DN)
to (305.58*( 525.+460.))*((0.002669* 118.)»( 33.002* ,992*( 29.81*( .699/13.6))/( 65.+460.)))
-J ISO » ————————————————— ...... —....................................... B 124.23 PEHCf.M
60. • 18.72 • 29.72 * .398 * .398
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 • MN • 15.43 / VMSTO
CS * 0.001 * .0 • 15.43 / 32.972 s .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR a CS * OSSTD / (15.43 * 453.6)
PMR « .000 * 15*2934. / (15.43 * 453.6) « .00
-------
Run No. 4.3
Sample volume =0.93 m3.32.97 scf
Example calculations
CS (Part) =61.1 /1.93= 65.7 ma/m3
CS (Part) = 0.001 x61.1 x 15.43/32.97=0.028 qr/dscf
CS (S02) =1250/0.93=1344 ma/m3
= 1344 x 24.06/64 = 505 ppm
= 0.001 x 1250 x IS.43/22*32- = JL585 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
61.1
6.4
8.7
1250
29.8
2 Concentration,
mg/m
65.7
6.9
9.4
1344
32.0
gr/dscf
0.028
0.003
0.004
0.585
0.014
ppm
505
8
A-138
-------
FIELD DATA
OJ
vo
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 4-4-M8-400
OPERATOR CLARKE
AMBIENT TEMP. (OEG.F) 56.
BAR. PRESS. (IN. HG) 26.01
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530069
STACK INSIDE DIM. (IN) 97. SO .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 5.0 IN.MG
METER CALIB. FACTOR 1.016
READ ft RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INlf
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
55.0
60.0
TIME
(24-HR
f»i nf tf )
ILUEK/
1543
1553
1603
1613
1623
1633
1708
1715
READING
(CU.FT.)
6.355
11.050
15.885
20.586
25.371
29.486
34.987
37.334
HEAD
(IN.H20)
—
.060
.060
.060
.060
.060
.070
.030
DIFFERENTIAL
(IN.
DESIRED
.74
.74
.74
.74
.74
.82
.37
H20)
ACTUAL
.74
.74
.74
.74
.74
.02
.37
STACK
TEKP
(DEG.F)
547.
556.
515.
521.
532.
519.
515.
DATE 10/28/81
NUN NUMBER 4-4
PHOBE LENGTH ft TYPE 5 FT GLASS HEAlEU
NOZZLE : 1.0. .397
ASSUMED MOISTURE 12.0
SAKPLE BOX NUMBER
PETER BUX NUMBER FB5
HE1ER HEAD DIFF. 1.86
C FACTOR .88
HHOBE HEATER SETTING 400.
HEATER BOX SETTING 400.
REFERENCE PRESS. DIFF. 1.50
OHY GAS METER PUMP SAMPLE IMPINGEH
TEMP
(DEG
INLET
69.
70.
74.
78.
HI.
82.
77.
.F)
OUTLET
70.
70.
70.
70.
72.
72.
74.
VACUUM
(IN.HG)
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(OEG.F)
275.
355.
342.
312.
325.
363.
386.
TEMP
(DEG.F)
46.
42.
4U.
40.
47.
44.
58.
TOTALS
AVERAGE
60.0
30.979
,70
,70 529.
76.
71,
1.0
337.
45.
-------
PARTICIPATE FIELD DATA « RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
4-4
COKE OVEN OUTLET
I
O
TEST
TB
TF
TT
NP
Y
DN
CP
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
ENGLISH UNITS
10/28/61
1543
1715
60.0
7
1.016
.397 IN
.84
METRIC UNITS
10/28/61
1543
1715
60.0
7
1.016
10.1
.84
KM
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTO VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL HZO COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRV
POZ PERCENT 02 BY VOL., DRV
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRV
MO MOLECULAR MT-ORY STACK GAS
MM3 MOLECULAR NT-STACK GAS
.70 IN-H20
30.979 CU-FT
17.7 CM-H20
.877 CU-M
73.
30.
166.
5.
If.
•
4.
11.
•
84.
'29.
27.
5 F
048 SCF
5
013 SCF
30
657
10
00
00
90
10
51
23.
•
106.
•
14.
•
4.
11.
•
84.
29.
27.
1 C
851 SCC
s
142 SCH
30
857
10
00
00
90
10
51
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK 6*3
PS STACK PRESr ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
Q3STD STACK FLOM RATE, DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DE6 F, 24.92 IN.HG.
28.81 IN-HG
•1.20 IN-H20
28.72 IN-HG
529. F
19.1 FPS
SO-IN
SCFM
ACFH
7466.
1564464.
3562981.
115.9
.0
731.77 fM-HG
-30. 4« C
789.53 PM-HG
276. C
5.8 KPS
4.817 SO-M
44301. SCMH
100893. *CCM
115.9
.0
.0000 GR/OSCF*
.000 LB/HK
.000
.00 KG/HK
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 0-«
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VM3TO • (17.647 • VM * T • (PB * PM / IS.6)) / (TM * 460.)
17.647 * 30.979 * 1.016 * ( 28.61 » .699 / 13.6)
VMSTO * ——————.......................... . . - 30.018 OSCF
I 74. » 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 • VLC
VMC • .04707 * 107. « 5.01 SCF
PERCENT MOISTURE IN STACK GAS
BMO «i~(id6. • ^fMC) / (VMSTD * VMC)
100. • 5.01
BMO • —————————— = 14.30 PERCENT
jp 30.046 * 5.01
H .... -
a*.
10 MOLE FRACTION OF CRT STACK GAS
FMD « (100. - BMO) / 100.
100. - ~14.3
FMD • ——— — s .857
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MO * (PC03 * .44) * (POZ * .32) * (PN3 » PCO) * .28
MD • ( 4.10*44/100) * (11.0*32/100) * ((80.9* .0) * 28/100 r 29.10
MOLECULAR HEIGHT OF STACK GAS
MMS • MD * (1. - (BMO/100)) » 16. * (BMO/100)
MMS * Z9.10* (1. -(14.30/100)) * 16. • (14.30/100) a 27.51
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OECP « SUM. OF THE SQRT(VH * (T3 + 460.))
VS * 65. 49 • CP * DELP / (SURT(MNS * PS) * PNTS)
VS » 85.49 • .84 * 52.303 / ISQRU 27.51 • 28.72) * 7. r 19.09 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS * 19.09 • ?466. 3600/144 3 3562981. ACFH
STACK GAS VOLUMETRIC FLOM AT STANDARD CONDITIONS
OSSTO • 17.647 • OS * PS * (1. - (BMO/iffO)') / (TS » 460.)
17.647 • 3562981. • 28.72 * (1. - (14.30/100))
OSSTO * —————— —————— — — --- - r 1564464. SCFH
( 529. «• 460.)
PERCENT ISOKINETIC
ISO • (305.S8«(TS*460.))«((0.002669«VLC)»(VH*V«(PB»(PW/13.6) ) / (TM«460.) ) ) / (TT*VS*PS*DN*DN)
(305. 5S*t S29. +460. ))*((0. 002669* 107.)+( 30.979*1 .Ol6*( 28.81M .699/13.6) )/( 74.«460.)))
ISO » — - --- — --- — — — — — --- — — — — ----------------------------- — ------- — ------- . --- 3 115.86 PEHCENT
60. • 19.09 • 2B.72 • .397 • .3V7
PARtfCULATE LOADTNe— EPA METHOD 5 «T STANDARD CONDITIONS)
CS • 0.001 • MN * 15.43 / VMSTD
CS » 0.001 * .0 • 15.43 / 30.048 a .000 GR/DSCF
PART1CULATE LBS/HR " EPA METHOD 5
PMR • CS * QSSTD / (15.43 * 453.6)
PMR « .000 * 1564464. / (15.43 • 453.6) = .00
-------
Run No. 4.4
3
Sample volume =0.85 m t 30.OR scf
Example calculations
CS (Part) =78.4/0.85 = 92.2 ma/m3
CS (Part) = 0.001 x78.4 x 15.43/30.05 - 0.040 qr/dscf
3
CS (S02) =1160/0.85 = 1364 mg/nT
= 1364 x 24.06^4 = 513ppm
= 0.001 xl160 x 15.43/_2O5_
0.596 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
78.4
12.6
17.2
1160
10.4
3 Concentration,
mg/m
92.2
14.8
20.3
1365
12.2
gr/dscf
0.040
0.006
0.009
0.596
0.005
PPm
513
3
A-144
-------
FIELD DATA
M
*»
Ul
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE STACK
SAMPLE TYPE METHOD 5-230
OPERATOR DO/MP
AMBIENT TEMP.(DEG.F) 58.
BAR. PRESS. (IN.HG) 29.81
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530026
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 8 11.
METER CALI8. FACTOR 1.033
READ ft RECORD DATA
TRAVERSE SAMPLE
POINT TIME
NO. (MIN.)
INtT t '-
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
130.0
140.0
150.0
CLOCK
TIME
(24-HR
1423
1433
1443
1453
1503
1513
1523
1533
1543
1553
1603
1613
1623
1633
1643
1706
EVERY iO.O
GAS METER
READING
(CU.FT.)
77*. 364
764.300
769.220
794.140
799.100
604.000
606.930
613.660
618.830
823.770
628.690
633.660
636.580
643.550
646.497
653.407
MINUTES
VELOCITY
HEAD
(IN.H20)
.073
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
.075
CLEVELAND
5 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.81
.81
.61
.61
.61
.61
.81
.81
.61
.61
.61
.61
.61
.61
.81
H20)
ACTUAL
.at
.81
.61
.61
.61
.61
.61
.61
.81
.81
.81
.81
.81
.81
.61
STACK
TEPP
(DEG.F)
916.
516.
518.
516.
516.
516.
516.
516.
516.
516.
518.
516.
516.
516.
516.
DATE 10/28/81
RUN NUMBER 0-5
PROBE LENGTH ft TYPE 6* GLASS
NOZZLE 1 I.D. .377
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBER FB4
PETER HEAD DIFF. 1.68
C FACTOR .92
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .17
DRV GAS METER
TEMP
(OEG.P)
INLET OUTLET
64. 62.
65. 62.
66. 62.
67. 62.
68. 62.
68. 62.
67. 62.
67. 62.
67. 62.
67. 62.
66. 62.
68. 62.
67. 62.
66. 62.
67. 64.
PUMP
VACUUM
(IN.HG)
a.
9.
10.
10.
10.
10.
11.2
10.6
10.7
10.5
11.0
10.6
10.7
10.6
10.4
SAMPLE
BOX TEMP
(OEG.F)
237.
255.
274.
266.
244.
262.
27.5.
275.
272.
274.
270.
27.3.
27.5.
273.
254.
IMPINGER
TEMP
(OEG.F)
47.
47.
18.
46.
44.
SO.
47.
46.
45.
46.
46.
•6.
46.
46.
46.
TOTALS
AVERAGE
150.0
74.041
.61
.81 318.
67.
62.
10.6 265.
-------
PARTICIPATE FIELD DATA B RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND 00/MP
TEST
••5
COKE STACK
TEST DATE
ENGLISH UNITS
10/28/61
METRIC UNITS
10/26/61
TB
TF
TT
NP
¥
DN
CP
PM
TIME-START
TIME-FINISH
NET TIME OF TEST* MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
1423
1706
150
15
1
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL*ML.
VNC VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.r DRV
P02 PERCENT 02 BY VOL.* DRV
PCO PERCENT CO BY VOL.* DRY
PN2 PERCENT N2 BY VOL.* DRY
MD MOLECULAR NT-DRY STACK GAS
MMS MOLECULAR NT-STACK GAS
1.033
.377 IN
.84
.61 IN-H20
74.041 CU-FT
64.5 F
76.660 SCF
280.7
13.213 SCF
1706
150.0
15
1.033
9.6 MM
.64
20.6 MM-H20
2.097 CU-M
16.1 C
2.176 SCM
280.7
.374 SCM
14.67
.653
4.10
11.00
.00
84.90
29.10
27.47
14.67
.853
4.10
11.00
.00
84.90
29.10
27.47
-------
PB BAROMETRIC PRESSURE
PSi STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE* DRY*
03 ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINCTIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
29.81 IN-HG
•1.20 1N-H20
29.72 IN-HG
518. F
21.5 FPS
7466. 30-IN
1838631. SCFH
401772S. ACFN
111.8
.0
.0000 GR/OSCF*
.000 LB/HR
757.17 MM-MG
•30.48 MM-H20
754.93 MM-HG
270. C
6.6 «PS
4.817 SO-M
52065. 3C»H
113770. »CHH
111.8
.0
.000 PG/OSC*
.00 KG/HR
* 66 DEC F,
IN.H6.
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 4*5
COKE STACK
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.647 • VM * V • (PB • PM / 13.6)) / (TM * 460.)
17.647 • 74.041 * 1.033 • ( 29.81 * .810 / 13.6)
VMSTD » ••-—-..—.—.——............................... • 76.860 DSCF
( 65. * 460.)
VOLUME OF NATER VAPOR AT STANDARD CONDITIONS
VHC « .04707 * VLC
VHC « .04707 * 281. » 13.21 SCF
PERCENT MOISTURE IN STACK GAS
"~ Stid • UOlT. • VHC) / (VM3TO * VHC)
100. * 13.21
> BHO « .————.———.— ;« 14.67 PERCENT
I 76.860 * 13.21
M
00
MOLE FRACTION OF DRY STACK GAS
FMD • (100. • BNO) / 100.
100. - 14.7
FMD « -————.-—..— • .853
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO « (PC02 * .44) » (P02 * .32) » (PN2 • PCO) • .28
MD • ( 4.10*44/100) * (11.0*32/100) * ((84.9* .0) * 28/100 » 29.10
MOLECULAR HEIGHT OF STACK GAS
MHS * MD * (1. • (BMO/100)) » 18. * (BHO/100)
MHS « 29.10* (1. -(14.67/100)) » 18. * (14.67/100) • 27.47
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. Or THE SQRTtVH * (TS » 460.))
VS « 65.49 • CP • OELP / (SORT(MW3 • PS) • PNTS)
VS « 85.49 * .84 * 128.467 / (SORT( 27.47 • 29.72) • 15. • 21.52 FPS
STACK 6A8 VOLUMETRIC FLO* AT STACK CONDITIONS
OS » VS * AS • 3600/144
OS « 21.5* • 7466. 3600/144 » 4017725. ACFH
STACK CAS VOLUMETRIC FLO* AT STANDARD CONDITIONS
093TO « 17.647 • OS * PS • (1. - (8MO/100)) / (TS * 460.)
17.647 * 4017725. • 29.72 • (1. • (14.67/100))
OSSTD • ..————————.—————................ • 1838631. 3CFH
( 518. * 460.)
I PERCENT ISOKINETIC
M
£ ISO • (305.58*(TS*460.))*((0.002669«VLC)»(VN*Y»(PB*(PM/13.6))/(TM*460.)))/(TT»VS*P8*DN«DN)
(305.50*( 518.»460.))«C(0.002669* 281.)*( 74.041*1.033*1 29.81«( .810/13.6))/( 65.4460.)))
130 • [[[ • 1U.85 PERCENT
ISO. • 21.52 • 29.72 • .377 • .377
PANICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 • MN • 15.43 / VMSTD
CS » 0.001 • .0 • 15.43 / 76.860 • .000 6R/D8CF
PARTICULATE LBS/HR — EPA METHOD 5
-------
Run No. 4.5
Q
Sample volume = 2.18 m . 76.86 scf
Example calculations
CS (Part) =174.5/2.18 = 80.0 mq/m3
CS (Part) = 0.001 x 174.5X 15.43/76.86
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/
0.035 gr/dscf
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
174.5
137.3
128.8
112.4
104.7
99.0
0.0
0.0
65.7
3.1
14.3
o Concentration,
mg/m
80.0
63.0
59.1
51.6
48.0
45.4
0.0
0.0
30.1
1.4
6.6 j
gr/dscf
0.035
0.028
0.026
0.022
0.021
0.020
0.0
0.0
0.013
0.001
0.003
ppm
A-150
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(OEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.M20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
READ • RECORD DATA EVERT
REPUBLIC STEEL CLEVELAND
COKE STACK
METHOD 8-600
DO/MP
58.
29.01
•1.20
3530226/3530206
97.50 .00
.84
.000 CFM 3 20.0 IN.HG
.982
10.0 MINUTES
DATE 10/28/81
RUN NUMBER 0-6
PROBE LENGTH ft TYPE a* UUAHTZ
NUZZLE : I.D. .620
ASSUMED MOISTURE 11.0
SAPPLE BOX NUMBER
PETER BOX NUMBER FBB
PETER MEAD OIFF. 1.91
C FACTOR .91
PROBE HEATER SETTING 600.
HEATER BOX SETTING 600.
REFERENCE PRESS. OIFF. .02
>
M
(Jl
I-1
TRAVERSE SAMPLE
POINT TIME
NO. (MIN.)
INlf" 0
10.0
20.0
30.0
40.0
50.0
60.0
ro.o
60. 0
90.0
100.0
110.0
CLOCK
TIME~
(24-HR
n ftp if i
vLUlfK 9
T«2?
1437
1447
1457
1507
1517
1527
1537
1547
1557
1714
1716
GAS METER
READING
(CU.FT.)
269.548
274.840
278.700
282.500
286.360
290.190
294.0)0
297.530
300.570
303.500
308.180
309.023
VELOCITY
HEAD
(IN.H2U)
.....
.075
.075
.075
.075
.075
~ .075
.075
.075
.075
.075
.075
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
5.73
5.73
5.73
5.73
5.73
5.73
5.73
5.73
5.73
5.73
5.73
H20)
ACTUAL
1.00
.50
.50
.50
.50
.50
.40
.30
.30
.75
.75
STACK
TEMP
(OEG.F)
518.
518.
518.
518.
518.
518.
518.
518.
518.
518.
518.
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
58. 56.
60. 56.
63. 57.
64. 57.
65. 58.
66. 58.
67. 59.
68. 60.
69. 61.
66. 63.
66. 61.
PUMP
VACUUM
(IN.HG)
5.5
10.6
13.3
16.2
18.2
19.5
21.5
21.3
23.3
3.7
3.8
SAPPLE
BOX TEMP
(DEG.F)
586.
596.
606.
630.
642.
620.
620.
627.
631.
621.
663.
IPPINGEH
TEMP
(DEG.F)
38.
36.
38.
38.
40.
42.
44.
49.
43.
46.
38.
TOTALS
AVERAGE
110.0
39.475
5.73
.55 518.
65.
59.
14.3
622.
41,
-------
PARTICULAR FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO/MP
TEST
4-6
COKE STACK
Ln
NJ
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
10/28/61
14*7
1716
110
11
.0
.962
.620 IN
.64
.55 IN-H20
METRIC UNITS
10/28/61
1427
1716
110
11
15
13
.0
.982
.7
.84
.9
KM
KM-
DROP
VM VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC "" TOTAL' HZO"COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRV GAS
PC02 PERCENT C02 BY VOL.* DRY
P02 PERCENT 02 BY VOliY D*Y
PCO PERCENT CO BV VOL.» DRV
PN2 PERCENT N2 BV VOL., DRY
MO 'MOLECULAR IT-DRY STACK GAS
MHS MOLECULAR NT-STACK GAS
39.475 CU-FT
61.7 F
39.139 SCF
Il9.4
6.091 SCF
1.116 CU-M
16.5 C
1.106 SCM
129.4
.172 SCM
13.47
.665
4.10
n.oo
.00
B4.90
"Z^.iO
27.60
13.47
.865
4.10
11.00
.00
64.90
29.10
27.60
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
V8 AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE, DRY*
US ACTUAL STACK FLO* RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 3
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 6* OE6 F, 29.92 IN.M6.
29.61 IN-HG
-1.20 IN-H2U
29.72 IN-HG
516. F
^1.5 FPS
7466. SO-IN
1660026. SCFH
4006004. ACFH
26.4
.0
.0000 GR/DSCF*
.000 LB/HH
757.17 >«M-HG
-30. «8 PK-H20
754.9J VM-HG
270. C
6.5 *PS
4.617 SU-M
52670. 3CI"H
113495. ACHH
26.4
.0
.000
.00 KG/HH
Ul
CO
-------
Ul
*»
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 4-6
COKE STACK
VOLUME OF DRY 6AS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.647 * VM * Y • (PB * PM / 13.6)) / (TM + 460.)
17.647 * 39.475 • .962 • ( 29.81 * .545 / 13.6)
VMSTD « "— —....—. .............. « 39.139 DSCF
( 62. » 460.)
VOLUME OF HATER VAPOR A'T STANDARD CONDITIONS
VMC • .04707 • VLC
VWC i .04707 * 129. « 6.09 SCF
PERCENT MOISTURE IN STACK CAS
BMO « (100. •VWC)/ (VMSTD * VMC)
100. * 6.09
BMO » —• —— ......... m 13.47 PERCENT
39.139 * 6.09
MOLE FRACTION OF DRY STACK GAS
FMD • (100. • BMO) / 100.
100. - 13.5
FMD • ————— ———— z .865
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO = (PC02 * .44) * (P02 * .32) * (PN2 * PCU) * .28
MD * ( 4.10*44/100) * (11.0*32/100) » ((84.9* .0) * 28/100 = 29.10
MOLECULAR HEIGHT OF STACK GAS
MMS « MO * (1. - (BMO/10U)) » 18. * (BMO/100)
MHS « 29.10* (1. -(13.47/100)) » 18. * 113.47/100) s 27.60
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE SQRT(VH * ITS » 460.))
VS « 65.49 * CP * DELP / (SORT(MHS • PS) * PNTS)
V3 « 85.49 * .84 • 94.209 / (SORT( 27.60 • 29.72) • 11. = 21.17 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS s VS * AS * 3600/144
OS • Z1.47 * 7466. 3600/144 • 4008004. ACFH
STACK 6AS VOLUMETRIC FLOM AT STANDARD CONDITIONS
QSSTD « 17.607 * OS * PS * U. - (BltO/lOO)) / (TS * 460.)
17.647 * 4008004. * 29.72 * (1. - (13.47/100))
OSSTO « —————— — — ..——.———..—. . = 1060026. SCFH
I 518. * 460.)
*f PERCENT ISOKINETIC
M
£ ISO • (305.58«(T3*460.))*l(0.002669«VLC)«(VM«YMPB+(PM/13.6))/(TM + .00
-------
Run No. 4.6
Sample volume =1.11 m ,39.14 scf
Example calculations
CS (Part) = 69.7/1.11 = 62.8 mq/m3
CS (Part) = 0.001 x 69.7 x 15.43/39.14 = 0.027 qr/dscf
CS (S02) = 1550/1.11 = 1396 mg/m3
= 1396 x 24.06/_6J_=_5Z5ppm
= 0.001 x 1550 x 15.43/3HU4_ = n.fill gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
69.7
0.0
0.0
1550
73.7
, Concentration,
mg/m
62.8
0.0
0.0
1396
66.4
gr/dscf
0.027
0.0
0.0
0.611
0.029
ppm
525
16.3
A-156
-------
FIELD DAT*
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING-LOCATION N01 COKE BATTERY OUTLE1
SAMPLE TYPE PART/S02/H2S04
OPERATOR BRUFFEY
AMBIENT TEMP. (OEG.F) 52.
BAR. PRESS. (IN.HG) 29.66
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530071
STACK INSIDE DIM. (IN) 97.50 .00
P1TOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 3 6.0 IN.HG
METER CALIB. FACTOR 1.003
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INlt
TIME
(MIN.)
6
10.0
20.0
30.0
40.0
50.0
60.0
70.0
60.0
90.0
100.0
110.0
114.9
TIME
(24-HR
940
950
1000
1010
1020
1030
1040
1050
1100
1110
1120
1130
1137
READING
(CU.FT.)
873.366
676.400
883.410
866.430
893.040
896.110
903.100
907.750
912.410
916.700
923.380
926.100
930.347
HEAD
(IN.H20)
.060
.060
.060
.050
.060
.060
.050
.050
.100
.050
.050
.050
DIFFERENTIAL
(IN.
UESIRfcU
.73
.73
.73
.62
.73
.73
.62
.62
1.22
.62
.62
.62
H20)
ACTUAL
.73
.73
.73
.62
.73
.73
.62
.62
1.22
.62
.62
.62
STACK
TEMP
(DEG.F)
530.
543.
556.
518.
529.
495.
531.
545.
501.
519.
530.
495.
DATE 10/29/81
RUN NUMBER 5-1
PROBE LENGTH ft TYPE 5* HEATEU GLASS
NOZZLE : I.U. .390
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER 0
MtTER BOX NUMBER FB2
KETER HEAD OIFF. 1.76
C FACTOR .86
PROBE HfcATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .15
UkY GAS METER PUMP SAMPLE IMPINGER
TEMP
(DEC
INLET
52.
54.
56.
62.
63.
64.
66.
67.
68.
69.
69.
70.
.F)
OUTLET
52.
52.
52.
53.
54.
56.
56.
58.
59.
60.
61.
62.
VACUUM
(IN.HG)
2.0
3.0
3.0
2.5
2.5
2.5
2.0
2.5
2.5
3.5
4.0
3.0
BOX TEMP
(DEG.F)
227.
263.
259.
258.
264.
260.
254.
251.
255.
260.
252.
255.
TEMP
(OEG.F)
41.
40.
41 .
42.
41.
42.
46.
48.
49.
52.
57.
56.
TOTALS
AVERAGE
114.9
56.961
.72
.72 524.
64.
56.
2.8 255.
46.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFET
TEST
3-1
N01 COKE BATTERY OUTLET
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
DN
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
10/29/81
940
1137
110
12
1
.9
.003
.398 IN
.84
.72 IN-H20
METRIC UNITS
10/29/81
940
1137
114
12
1
10
18
.9
.003
.1
.84
.2
KM
KM-
•f DROP
Ln VM VOLUME OF DRV GAS SAMPLED
0° AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H2o COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
8*0 PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRY
P02 PERCENT 02 BY VOL., DRV
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRV
MD MOLECULAR MT-ORY STACK GAS
MWS MOLECULAR MT-STACK GAS
56.981 CU-FT
59.9 F
58.031 SCF
.1
8.901 SCF
1.614 CU-M
15.5 C
1.643 SCK
189.1
.252
13.30
.867
4.30
11.30
.00
84.40
29.14
27.66
13.30
.867
4.30
11.30
.00
84.40
29.14
27.66
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRE3 OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
03STD STACK FLOW RATE* DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 29.92 IN.HG.
29.86
-1.20
29.77
S24.
18.9
7466.
1628613.
3519316.
111.7
.0
IN-HG
IN-H20
IN-HG
F
FPS
SQ-IN
SCFH
ACFH
.0000 GR/DSCF*
.000
LB/HR
758.44
-30. 4B
756.20
274.
5.7
4.817
46117.
99656.
111.7
.0
.000
.00
CM-HG
*M-H20
»N-HG
C
*P3
30-M
SCMH
»C*H
VG/DSCI
KG/HH
Ul
VO
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 5-1
N01 COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.647 * VM * Y * (PB * PM / 1J.6)) / (TM «• 460.)
17.647 • 56.981 « 1.003 * ( 29.86 * .716 / 13.6)
VMSTD * ————————*-— — — - — - — ---- — ..... - 58.031 OSCF
( 60. + 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC » .04707 * VLC
VWC * .04707 • 18$. » 8;«*0 SCF
PERCENT MOISTURE IN STACK GAS
BMO « (100. * VMC) / (VMSTD * VWCJ
100. • 8.90
BMO = ————————— > 13.30 PERCENT
> SB.031 * B.90
O
MOLE FRACTION OF DRY STACK GAS
FMD * (100. • BMO) / 100.
10
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE SQRT(VH * (TS » 460.))
VS 3 SS.49 • CP • DELP / (SQRT(MMS * PS) * PNTS)
VS • 05.49 * .84 • 90.411 / (SORT( 87.66 • 29.77) * 12. = 18.65 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS > VS * AS • 3600/144
OS « 18.85 • 7466. 3600/144 • 3519316. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
03STD « 17.647 • OS • PS • (1. - (BMO/166)) / (TS * 460.)
17.647 • 3519316. * 29.77 * (1. • (13.30/100))
QSSTD = ——--————-—— — — --——— ——— s 1628613. SCFH
( 524. «• 460.)
PERCENT ISOKINETIC
>
jL ISO • (305.5S*(TS«460.))*((0.002669*VLC)«(VM*Y*(PB«(PM/13.6))/(TM4460.)))/(TT*VS*PS*DN*DN)
CTl _
H (305.S0*( 524.*460.))*((0.002669* 109.)+( 56.981*t.003*( 29.06*( .716/13.6))/( 60.4460.)))
ISO * ...... ......... ... ........ ....... ....... s 111.67 PERCENT
115. * 18.85 • 29.77 * .390 * .340
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTO
CS * 0.001 * .0 * 15.43 / 58.031 * .000 GR/DSCF
PARTICULATE LBS/MR — EPA METHOD 5
PMR « CS • OSSTO / (15.43 * 453.6)
PMR • .000 * 1620613. / (15.43 • 453.6) = .00
-------
Run No. 5.1
Sample volume =1.64 m3. 58.03 scf
Example calculations
CS (Part) =138.6/1.64 = 84.5 mq/m3
CS (Part) = 0.001 x138.6x 15.43/ 58.03= 0.037 qr/dscf
3
CS (S02) =2070/1.64= 1262mg/nT
= 1262 x 24.06/64 = 474 ppm
= 0.001 x2070 x 15.43/58.03
0.550 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
138.6
85.6
117.0
2070
34.4
3 Concentration,
mg/m
84.5
52.2
71.3
1262
21.0
gr/dscf
0.037
0.023
0.031
0.550
0.009
ppm
474
5
A-162
-------
FIELD DATA
CTl
U)
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PANT
OPERATOR BRUFFEY
AMBIENT TEMP. (DEC. F) 52.
BAR. PRESS. (IN. HG) 29.86
STATIC PRESS. (IN. HZO) -1.20
FILTER NUMBER(S) 3530113
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .011 CFM 3 23.0 IN.HG
METER CALIB. FACTOR 1.004
READ & RECORD DATA EVERT 10.0 MINUTES
TRAVERSE
POINT
NO.
1NIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
CLOCK
TIME
(24-HR
pi nr v i
ILUtn J
943
953
1003
1013
1023
1033
1043
1053
1103
1113
1123
1133
GAS METER
READING
(CU.FT.)
101.037
105.700
110.380
115.030
119.330
123.990
128.300
132.610
136.900
142.830
147.070
151.348
VELOCITY
HEAD
(IN.H20)
.060
.060
.060
.050
.060
.050
.050
.050
.200
.050
.050
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.73
.73
.73
.62
.73
.62
.62
.62
1.22
.62
.62
H20)
ACTUAL
.73
.73
.73
.62
.73
.62
.62
.62
1.22
.62
.62
STACK
TEfP
IDEG.F)
536.
548.
507.
520.
533.
521.
536.
549.
510.
522.
536.
DATE 10/29/81
HUN NUMBER 5-2
PHUBE LENGTH S TYPE 4* HEATED GLASS
NOZZLE : I.I). .397
ASSUMED MOISTURE 12.0
SAMPLE BUX NUKBER 0
CETEH BOX NUMBtH F10
HETER HEAD D1FF. 1.80
C FACTOR .86
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. OIFF. .15
DRY GAS METER
TEMP
(OkG.F)
INLET OUTLET
58. 58.
60. 58.
b2. 58.
66. 60.
67. 61.
69. 61.
70. 63.
71. 64.
72. 65.
75. 66.
75. 67.
PUHP
VACUUM
(IN.HG)
2.0
2.5
2.0
2.5
3.0
3.0
2.5
3.0
3.0
4.0
8.0
SAMPLE
BOX TEMP
(UEG.F)
261.
270.
253.
253.
252.
251.
246.
251.
250.
256.
249.
IMPINGEW
TEMP
(DEG.F)
40.
40.
4U.
42.
43.
42.
47.
49.
51.
50.
55.
TOTALS
AVERAGE
110.0
50.311
.71
.71
529.
68,
62.
3.2 254.
45,
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
5-2
NO.l COKE BATTERY OUTLET
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
DN
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
10/29/81
443
1133
110
11
1
_
.0
.044
.397 IN
.64
.71 IN-H20
METRIC UNITS
10/29/61
943
1133
110
11
1
10
16
.0
.044
.1
.84
.1
KM
PM-I
DROP
VM VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
VLC '" TOTAL HiO COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VHC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
8WO ~ PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRV GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR MT-ORY STACK GAS
MMS MOLECULAR XT-STACK GAS
50.311 CU-FT
64.6 F
52.630 SCF
6.256 SCF
1.425 CU-M
16.2 C
1.496 SCM
175.4
.234 SCM
13.52
.665
4.30
11.30
.00
84.40
29.14
27.63
13.52
.665
4.30
11.30
.00
84.40
29.14
27.63
-------
PB BAROMETRIC PRESSURE
PS1 STATIC PRES OF STACK GAS
PS STACK PRES* AB3.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
A8 STACK AREA
OSSTD STACK FLOW RATE. DRY*
OS ACTUAL STACK FLO* RATE
ISO PERCENT ISOKINETIC
MM FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 29.92 iN.HG.
29.86 IN-HG
•1.20 IN-H20
29.77 IN-HG
529. F
19.8 FPS
7466. SO-IN
1698186. SCFH
3695966. ACFH
102.4
.0
.0000 GR/DSCF*
.000 LR/HR
758.44 PM-HG
-iO.46 P
756.20 fM-HG
276. C
6.0 fPS
4.617 3U-M
4A088. SCCH
104659. *CKH
102.4
.0
.000 PG/DSC*
.00 KG/Hk
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 5-2
NO.l COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDAHD CONDITIONS
VMSTD » (17.647 • VM * Y • (PB + PM / 13i6)) / (TM «• 060.)
17.647 • SO.311 « 1.044 * ( 29.86 * .715 / 13.6)
VMSTO • ——————........................ .. . . - 52.830 OSCF
( 65. * 060.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC » .04707 * VLC
VNC « .04.707 * 17S. * 8.26 SCF
PERCENT MOISTURE IN STACK GAS
"" BNO » (100. * VHC)~7 (VMSTD * VNC)
100. • 8.26
jjy BNO « —————— ....... r 13.52 PERCENT
I 52.830 * 8.26
I-"
MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BMO) / 100.
100. - 13.5
FMD a ——————— • .865
100.
AVERAGE MOLECULAR HEIGHT OF DRV STACK GAS
MD « (PC02 • .44) * (P02 • .32) * (PN2 * PCO) * .28
MD « ( 4.30«44/100) * (11.3*32/100) * ((84.4* .0) * 28/100 = 29.14
MOLECULAR HEIGHT OF STACK GAS
MNS 3 MD * (1. - (BHO/100)) » 18. « (BNO/100)
MNS • 29.140 (l. .(13.52/100)) * 18. * (13.52/100) » 27.63
-------
STACK 6AS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE SORTIVH • ITS » 060.))
VS » 65.09 * CP * OELP / (SORT(MHS * PS) * PNTS)
VS « 65.49 * .84 « 66.999 / (SORT( 37.63 « 29.77) * 11. = 19.60 FP3
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS • AS • 3600/144
OS • 19.60 * 7466. 3600/144 a 3695966. ACFH
STACK 6AS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD » 17.647 • OS • PS • (1. - (6*0/100)) / (TS * 460.)
17.647 • 3695966. • 29.77 • (1. - (13.52/100))
OSSTD • ————— — — — —————— r 1690186. SCFH
I 529. «• 460.)
PERCENT ISOKINETIC
>
jL ISO « (305.58«(TS*460.))M(0.002669«VLC)*(VM«Y»(PB*(PW/13.6))/(TM*460.)))MTT«VS*P9«DN*DN)
-J (305.58M 529.»460.))*t(0.002669* 175.)»( 50.311*1.044*( 29.86+( .715/13.6))/( 65.4460.)))
ISO * ..—————. .......... .. . .. . .... * 102.36 PtRCEM
110. * 19.80 • 29.77 * .397 • .397
PARTtCULATE LOAOlNfc — EPA METHOD 5 (Af STANDARD CONDITIONS)
CS > 0.001 * MN • 15.43 / VMSTO
CS > 0.001 * .0 * 15.43 / 52.630 e .000 GR/DSCF
PARTICIPATE LBS/HR — EPA METHOD 5
PMR • CS • QSSTD / (15.43 * 453.6)
PMR c .006 * 1696186. / (15.43 * 453.6) « .00
-------
Run No. 5.2
Sample volume = 1.50 m . 52.83 scf
Example calculations
CS (Part) = 185.6/ 1.50= 123.7 mq/m3
CS (Part) = 0.001 x 185.6 x 15.43/52.83 = 0.054 qr/dscf
3
CS (S02) = / = mg/m
= x 24.OS/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
185.6
36.8
3.0
4.1
19.0
4.2
58.1
2 Concentration,
mg/m
123.7
24.5
2.0
2.7
12.7
2.8
38.7
gr/dscf
0.054
0.011
0.0008
0.001
1
0.006
0.001
0.017
Ppm
A-168
-------
FIELD DATA
M
CT>
VO
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE S-3-MB-350
OPERATOR CLARKE
AMBIENT TEMP.(DEG.F) 52.
BAR. PRESS. (IN. HG) 29.06
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530073
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .04
THERM. NO.
LEAKAGE .000
METER CALIB. FACTOR .992
READ » RECORD DATA EVERY 10.0
TRAVERSE SAMPLE CLOCK GAS METER
POINT
NO.
IN if"'
TIME
(MIN.)
6
10.0
20.0
30.0
40.0
50.0
60.0
70.0
60.0
90.0
100.0
110.0
115.0
TIME
(24-HR
f i fif* tf t
LLUCK J
940
950
1000
1010
1020
1030
1040" "
1050
1100
1110
1120
1130
it35
READING
ICU.FT.)
616.015
621.635
626.300
631.020
635.502
639.909
644.604
649.300
653.003
659.305
663.440
666.370
670.591
CFM 8 3.
MINUTES
VELOCITY
HEAD
(IN.H20)
.060
.060
.060
.050
.060
.060
.050
.050
.100
.050
.050
.050
0 IN.HG
ORIFICE
PRESSUKE
DIFFERENTIAL
(IN.
DESIRED
.73
.T3
.73
.62
.73
.73
.62
.62
1.20
.62
.62
.62
H20)
ACTUAL
.73
.73
.73
.62
.73
.73
.62
.62
1.20
.62
.62
.62
STACK
TEI*P
(DEG.F)
DATE 10/29/01
HUN NUMBER b-3
PROBE LENGTH ft TYPE 5 FT GLASS HEATED
NUZZLE t I.D. .394
ASSUMED MOISTUHE 12.0
SAMPLE BOX NUMBER
PETER BOX NUMBER FBI
KETER HEAD DIFF. 1.87
C FACTOH .80
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
REFERENCE PRESS. OIFF. 1.50
OHY GAS METEH PUMP SAMPLE IMPINGEH
TEMP
IOEG.F)
VACUUM
(IN.HG)
BOX TEMP
(OEG.F)
TEMP
(OEG.F)
INLET OUTLET
530.
543.
556.
510.
530.
540.
531.
546.
505.
519.
530.
495.
55.
50.
60.
65.
67.
60.
70.
73.
76.
80.
00.
80.
SO.
51.
51.
52.
54.
54.
56.
60.
61.
64.
64.
64.
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.5
2.0
2.0
2.0
301.
362.
352.
342.
356.
358.
350.
359.
359.
354.
340.
351.
50.
44.
««.
48.
50.
56.
58.
52.
5o.
52.
56.
54.
TOTALS
AVERAGE
115.0
53.776
.71
,71
529.
69.
57,
2.0 349.
51,
-------
PARTICIPATE FIELD DATA A RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
5-3
COKE OVEN OUTLET
TEST DATE
TB
TF
TT
NP
V
ON
CP
PM
1 VM
O
TM
VMSTO
VLC
VNC
BHO
FMO
PC02
P02
PCO
PN2
MO
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL.* DRV
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/29/81
940
1135
115.0
12
.992
.394 IN
.84
.71 IN-H20
53.776 CU-FT
63.0 F
53.638 SCF
8.915 SCF
r«Y2i
.858
4.30
11.30
.00
84.40
-29. 10
27.56
METRIC UNITS
10/29/81
940
1135
115.0
12
.992
10.0
.84
18.1
1.523
17.2
1.525
189.4
.252
14.21
.858
4.30
11.30
.00
84.40
29.14
27.56
PM
MM-H2U
CU-M
c
SCM
SCM
-------
PB BAROMETRIC PRESSURE
P8I STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
A8 STACK AREA
Q33TD STACK FLON RATE, DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5 ________
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
29.86 IN-HG
-t.20 IN-H20
Z9.77 IN-HG
529. F
16.9 FPS
7066. 30-IN
1611199. SCFH
3533728. ACFH
106.8
.0
.0000 GR/OSCF*
.000 LB/HH
758.Ofl CM-HG
•30.08 PM-H2U
756.20 PM-HG
276. C
5.8 >»PS
a.817 SO-M
05620. 3CHH
100065. ACMH
106.6
.0
.000 fG/DSC"
.00 KG/HR
• 68 DEC F, 89.92! iN.MG.
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 5-3
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VM8TO • (IT.647 • VM * Y * (PB * PM / 1J.6)J / ITM * 460.)
17*647 • 53.776 * .992 * ( 29.86 * .714 / 13.6)
VMSTD « ——————.—————•———— ———-- = 53.838 DSCF
I 63. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC * .04707 * VLC
VNC • .04701 • f89. » "8.92 SCF
PERCENT MOISTURE IN STACK GAS
8NO » (100. • VNC) T (VMStO * VNC)
100. * 8.92
> BHO » ...... — ......... > 14.2i PERCENT
I 53.838 «• 8.92
(-•
NJ
MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BMO) / 100.
100."-~"H,Z "
FMD • —— ............... • .858
100.
AVERAGE MOLECULARHEIGHT OF D«Y STACK GAS
MO » (PC02 * .44) • (P02 • .32) » IPN2 4 PCO) * .28
MD * ( 4.30*44/100) 4 (11.3*32/100) * ((84.0* .0) * 28/100 * 29.14
MOLECULAR WEIGHT OF STACK GAS
MNS • MD * (1. - (BNO/100)) 4 18. * (BNO/100)
~ MNS « 29.14* (1. -(14.21/100)) « 18. * (14.21/100) a 27.56
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE 80RTCVH * US » 460.))
VS * 85.49 * CP * OELP / (SORMMHS * PS) * PNTS)
VS * 85.09 * .84 • 90.615 / (SORT( 27.56 * 29.77) * 12. s 18.93 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS • AS • 3600/144
OS • 18.93 • 7466. 3600/144 « 3533728. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTO • 17.647 * 03I • PS • (iT- (B«0/106j) / (TS «• 460.)
17.647 • 3533728. • 29.77 • (1. - (14.21/100))
OSSTO » ——————• —— ....... r 1611199. SCFH
( 529. + 460.)
PERCENT ISOKINETIC
ISO « (305.58MTS*460.))*((0.002669*VLC)+(V**Y*(PB+(PM/13.6))/(TM4460.)))/(TT*VS*PS*ON*ON)
(305.58*( 529V«46d.))*((0.002669l l89.)*l 53.776* ,992«( 29.86»( .7K/13.6) ) /( 63.«460.)))
ISO • .——.———— ........ ---- ........ --- ........ ------------ . ------ . ---- .... -------- .. -------- ... z 106.77 PEHCEN1
115. * 18.93 * 29.77 • .391 * .394
PARTICIPATE LOADING •• EPA METHOD 5 (At "STANDARD CBNDfTiONSl
CS « 0.001 * MN • 15.43 / VMSTO
CS « 0.001 * .0 * 15.43 / 53.838 * .000 GH/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR « CS * OSSTD / (15.43 * 453.6)
PMR « .600 • mtl99. / U5.43
-------
Run No. 5.3
Sample volume =1.53 m3r53.84 scf
Example calculations
CS (Part) =50.5 /I.53 = 33.0 ma/
m
CS (Part) = 0.001 x 50.5 x 15.43/53.84 = 0.014 qr/dscf
CS (S02) = 1970/1.53 = 1287 mg/m3
= 1287 x 24.06/64 = 484pom
= 0.001 x 1970 x 15.437 53.84 = O.B64 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04..2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
50.5
9.5
13.0
1970
81.5
- Concentration,
mg/m
33.0
6.2
8.5
1288
53.3
gr/dscf
0.014
0.003
0.004
0.564
0.023
ppm
484
13
A-174
-------
FIELD DATA
U1
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 5-4-MS-350
OPERATOR CLARKE
AMBIENT fEMP.TOE6.FJ 52.
BAR. PRESS. (IN. HG) 29.86
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER (3) 3530107
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 3.0 IN.HG
METER CALIB. FACTOR 1.016
READ * RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INlf
TIME
(MIN.)
0 "
10.0
20.0
30.0
ao.o
SO.O
60.0
70.0
80.0
90.0
100.0
110.0
112.0
TIME
(24-HR
n uric i
UUUln t
943
953
1003
1013
1023
1033
1043
1053
1103
1113
1123
1133
1135 ~
READING
(CU.FT.)
38.568
43.355
47.374
52.310
56.333
60.739
64.726
69.205
73.425
79.230
83.320
87.690
86.721
HEAD
(IN.H20)
.060
.060
.060
.050
.060
.050
.050
.050
.100
.050
.050
.050
DIFFERENTIAL
(IN.
DESIRED
.73
.73
.73
.62
.73
.62
.62
.62
1.20
.62
.62
.62
H20)
ACTUAL
.73
.73
.73
.62
.73
.62
.62
.62
1.20
.62
.62
.62
STACK
TEKP
(DEG.F)
536.
546.
507.
520.
531.
510.
535.
548.
510.
522.
536.
515.
DATE 10/27/81
RUN NUMBER 5-4
PROBE LENGTH ft TYPE 6 FT GLASS HEATED
NOZZLE < I.D. .396
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER 1
PETER BOX NUKBfcR FB5
PETER HEAD DIFF. 1.86
c FACTOR .88
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
HEFERENCE PRESS. DIFF. 1.50
DRY GAS METER PUMP SAMPLE IMPINGE"
TEMP VACUUM
(DEG
INLET
60.
61.
64.
68.
70.
74.
78.
80.
84.
87.
80.
69.
.F) (IN.HG)
OUTLET
60.
60.
60.
61.
63.
65.
68.
72.
75.
77.
80.
60.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(DEG.F)
300.
395.
377.
370.
363.
364.
364.
373.
371.
376.
367.
369.
TEMP
(OEG.F)
38.
38.
40.
40.
42.
46.
48.
46.
48.
50.
50.
46.
TOTALS
AVERAGE
112.0
50.153
.70
.70 527.
75.
66.
1.0 366.
45.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
COKE OVEN OUTLET
TEST DATE
TB
TF
TT
NP
V
ON
CP
PM
VM
TM
VMSTD
VLC
VHC
BMO
FMD
PC02
P02
PCO
PN2
MD
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
P1TOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 62 BY 'VOL., BUY
PERCENT CO BY VOL., DRV
PERCENT N2 BY VOL., DRV
MOLECULAft NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/27/81
943
1135
112.0
12
1.016
.396 IN
.84
.70 IN-H20
50.153 CU-FT
71.5 F
50.606 SCF
171.0
8.049 SCF
13.72
.863
4.30
11.30
.00
84.40
29.14
27.61
METRIC UNITS
10/27/81
943
1135
112.0
12
1.016
10.1
.84
17.9
1.420
21.9
1.433
171.0
.228
13.72
.863
4.30
11.30
.00
84.40
29.14
27.61
MM
*M-H
CU-M
c
SCM
SCH
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK CAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
Q3STO STACK FLOW RATE* DRY*
QS ACTUAL STACK FLOW RATE
ISO PERCENT I30KINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 PEG F> 24.92 IN.MG.
29.6b IN-HG
-1.20 IN-H2U
29.77 IN-HG
527. F
18.8 FPS
7466. SQ-IN
160837%. SCFH
3500352.
102.2
.0
ACFH
.0000 GR/DSCF*
.000 LB/HR
758. <4« CM-HG
-so. ae M
756.20 >>M-HG
275. C
5.T >»PS
4.817 30-M
assao. SCHH
99119. ACKIH
102.2
.0
.000
.00 KG/HH
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 5-4
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.647 * VM • T * (PB » PM / 13.6)) / (TM > 460.)
17.647 * 50.153 * 1.016 « ( 24.86 * .705 / 13.6)
VMSTD » ————————-—-——-—...... — = 50.606 DSCF
I 72. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VKC « .0*707 * VLC
VKC « .04707 * 171. a «U05~3CF
PERCENT MOISTURE IN STACK GAS
B*0 « (100. •"~VMC) / TVMSTD * VNC)
> too. * a.os
I BMO » ———— ........... * 13.72 PERCENT
^ 50.606 * 8.05
oo .
MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BNO) / 100.
~ 100. -13.7
FMO • .-.———————— 9 .863
100.
AVERAGE MOLECULAR WEI6HT OF DRY StACK GAS
MD * (PC02 * .44) • (P02 * .32) * (PN2 «• PCO) * .28
MO * ( 4.30*44/100) * (11.3*32/100) * ((84.0+ .0) * 28/100 = 29.14
MOLECULAR HEIGHT OF STACK GAS
MNS s MD * (1. - (BHO/100)) * IB. * (BMO/100)
MMS « 29.14* (1. -(13.72/100)) * 18. * (13.72/100) * 27.61
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP • SUM. OF THE SQRftVH • ITS » 460.))
VS • BS.49 • CP * OELP / (SORT(MHS * PS) * PNTS)
VS * 65.49 * .84 * 89.647 / (SORT! 27.bl • 29.77) * 12. = 10.75 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS • VS • AS * 3600/144
OS * 18.75 * 7466. 3600/144 s 3506352. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
03STO » 17.647 • OS * ~PS • U. - (BNO/100)) / (TS * 460.)
17.647 • 3500352. • 29.77 • 11. • (13.72/100))
QSSTO * -—.———— ———— —........ . ... = Ib0837b. SCFH
( 527. «• 460.)
> PERCENT ISOKINETIC
!~J ISO * (305.58*(TS*460.))«((0.002669*VLC)*(VM*Y*(PB*(PM/13.6))/(TM+460.)))/(TT«V3«P3«»DN*ON)
vo
(305.58»( 527.*460.))*((0.002669* 171.J*( 50.153*1.016*( 29.86*( .705/13.6))/( 72.+460.)))
ISO • ———•———.——.——.................................. ............................. s 102.19 PEHCEN1
112. * 18.75 * 29.77 • .396 * .396
PARflCULATE LOA6INB -S EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 • MN • 15.43 / VMSTD
CS * 0.001 * .0 • 15.43 / 50.606 s .000 GR/DSCF
PARTICIPATE LBS/HR " EPA METHOD 5
PMR * CS * OSSTD / (15.43 * 453.6)
PMR » .000 • 1608375. / (15.43 • 453.6) a .00
-------
Run No. 5.4
Sample volume = 1.43 m r 50.61 scf
Example calculations
CS (Part) = 32.I/ 1.43= 22.4 tna/m3
CS (Part) = 0.001 x 32.1 x 15.43/50.61
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.437
0.010 gr/dscf
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
32.1
0.0
0.0
101.2
3.2
49.2
2 Concentration,
mg/m
22.4
0.0
0.0
70.8
2.2
34.4
gr/dscf
0.010
0.0
0.0
0.031
0.001
0.015
ppm
A-180
-------
FIELD OAT*
00
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE STACK
SAMPLE TYPE METHOD 5-350
OPERATOR DO/MP
AMBIENT TEMP. (DEC. F) 52.
BAR. PRESS. UN. HG) 29.86
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530100
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .004 CFM 9 14.
METER CALIB. FACTOR 1.033
READ * RECORD DATA EVERY 10.0 MINUTES.
TRAVERSE
POINT
NO.
INI?
SAMPLE
TIME
(MIN.)
o
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
M3.7
CLOCK
TIME
(24-HR
PI nf*K i
ILUvn J
945 ~
953
1003
1013
1023
1033
1043
1053
1103
1113
1123
1133
1137
GAS METER
READING
(CU.FT.)
854.767
859.460
864.150
868.850
873.590
878.350
883.170
888.030
692.910
897.820
902.740
907.630
909.368
VELOCITY
HEAD
(IN.H20)
-
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
"" .070
CLEVELAND
0 IN.HG
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H20)
DESIRED ACTUAL
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
.72 .72
DATE 10/29/81
HUN NUMBER 5-5
PROBE LENGTH * TYPE 6* GLASS
NUZZLE I 1.0. .374
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
KETEH BOX NUMBER FB4
fETEH MEAD DIFF. 1.88
C FACTOR .92
PROBE HEATER SETTING 250.
HEATER BUX SETTING 250.
REFERENCE PRESS. I) IFF. .18
STACK
TE*P
(DEG.F)
520.
520.
520.
520.
520.
S20.
520.
520.
520.
520.
520.
520.
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
55. 54.
57. 55.
60. 56.
64. 56.
67. 60.
69. 62.
71. 64.
72. 66.
74. 68.
75. 69.
75. 70.
75. 71.
PUMP
VACUUM
(IN.HG)
0.7
8.7
8.8
.0
.0
.2
.6
.8
.9
10.1
10.7
12.2
SAMPLE
BOX TEMP
(OEG.F)
225.
244.
252.
246.
236.
243.
242.
236.
234.
240.
235.
841.
IMPINGER
TEMP
(DEG.F)
40.
40.
40.
41.
42.
44.
43.
44.
42.
42.
42.
44.
TOTALS
AVERAGE
113.7
54.601
.72
.72 520,
68.
63.
9.6 240.
42.
-------
PARTICIPATE FIELD DATA A RESULTS TABULATION
PLANT* NAME AND ADDRESS TESf TEAM LEADER
REPUBLIC STEEL CLEVELAND 00/MP
TEST
5-5
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1
M VM
00
N>
TM
VMSTD
VLC
VHC
BHO
FMD
PC02
P02
PCO
PN2
MO
MMS
TIME-STARf
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE CAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL.* DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR MT-ORY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/29/61
943
1137
113.7
12
1.033
.374 IN
.84
.72 IN-H20
54.601 CU-FT
65.3 F
56.660 SCF
197.2
9.282 SCF
14.07
.659
4.30
11.30
.00
84.40
" 29.14
27.57
METRIC UNITS
10/29/61
943
1137
113. 7
12
1.033
9.S
.84
18.3
1.546
18.5
1.605
197.2
.263
14.07
.659
4.30
11.30
.00
84.40
29.14
27.57
I'M
MM-H20
CU-M
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
P3I STATIC PRES OF STACK GAS
PS STACK PRES, A83.
TS AVERAGE STACK TEHP
VS AVG STACK GAS VELOCITY
AS STACK AREA
QSSTO STACK FLON RATE, ORT*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 39.93 IN.HG.
29.86 1M-HG
•1.30 1N-H30
29.77 IN-HG
520. f
20.8 FPS
7466. 30-IN
1785009. SCFH
3674661. ACFH
113.9
.0
.0000 GR/OSCF*
.000 LB/HR
758.44 CM-HG
-30.48 H
756.30 PM-HG
3M. C
6.3 CPS
a.817 SO-M
50546. SO'H
109734. ACK-H
113.9
.0
.000 PG/DSCP
.00 KG/HR
00
U)
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 5-5
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (It.647 • VM * Y * (PB * PM / 13.6)) / (TM + 460.)
17.647 * 54.601 • 1.033 * ( 29.86 » .720 / 13.6)
VMSTD « ———————— — — s 56.680 OSCF
( 65. » 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 • VLC
VMC • .04707 * 197. • 9.28 SCF
PERCENT MOISTURE IN STACK GAS
BMO » (100. * VMC) / (VMSTD «• VMC)
100. • 9.28
BNO « —— — ......... z 14.07 PERCENT
•f 56.680 * 9.28
t-1
CO
MOLE FRACTION OF DRV STACK GAS
FMD « (100. • BMO) / 100.
100. - 14.i~
FMD * — ————— x .859
100.
AVERAGE MOLECULAR HEIGHT OP DRY STACK GAS
MD * (PC02 * .44) * (P02 * .32) » (PN2 * PCO) * .28
MO * ( 4.30*44/100) • (11.3*32/100) + ((84.4» .0) * 28/100 z 29.14
MOLECULAR NEIGHT OF STACK GAS
MMS * MO • (1. • (8*0/100)) *• 18. * (BNO/100)
MMS • 29.14* (1. -(14.07/100)) + 18. * (14.07/100) * 27.57
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SQRUVH • (TS * 060.))
VS > 85.49 • CP * OELP / (SORT(MNS * PS) * PNTS)
VS > 65.49 * .84 • 99.390 / (SQRT( 27.57 * 29.77) * 12. = 20.76 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS * VS • AS * 3600/144
OS * 20.76 * 7466. 3600/144 a 3874861. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO * 17.647 * OS • PS •"(1. - (BNO/iOO)) / (TS * 460.)
17.647 • 3874861. • 29.77 • (1. • (14.07/100))
OSSTD « ——— — — — s 1765009. SCFH
( 520. * 460.)
> PERCENT ISOKINETIC
£ ISO • (305.58*(TS«460.))*((0.002669*VLC)+(VM«Y«(PB+(PM/13.6))/(TM»460.)))/ITT«V3«PS«ON«DN)
(305.58M «0.+460.))*((b.002669* 197.>+( 54.601*1.033*( 29.66«( .720/13.6))/( 65.+460.)))
ISO « ——————————————— — ...... —. . .. .. • U3.89 PERCENT
114. * 20.76 * 29.77 * .374 • .J74
PARTICIPATE LOADING —"EPA METHOD 5 (AT STANDARD CONDITIONS)
CS » 0.001 * MN * 15.43 / VMSTD
CS * 0.001 * .0 » 15.43 / 56.680 * .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR s CS • OSSTO / (15.43 * 453.6)
PMR * .000 * FfaSObT. / (15.43 • 453.6) s .00
-------
Run No. 5.5
Sample volume =1.61 m .56.68 scf
Example calculations
CS (Part) =221.0; 1>61. 137.3 mq/m3
CS (Part) = 0.001 x_22J_._Ox 15.43/ 56.68= 0.060 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = pptn
= 0.001 x . x 15.43/ = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
221.0
50.4
44.2
36.2
32.3
27.7
0.0
0.0
20.9
6.3
11.8
3 Concentration,
mg/m
137.3
31.3
27.4
22.5
20.1
17.2
0.0
0.0
13.0
3.9
7.3
gr/dscf
0.060
0.014
0.012
0.010
0.009
0.008
0.0
0.0
0.006
0.002
0.003
ppm
A-186
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DE6.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
CUKE STACK
METHOD 8-600
DO/MP
52.
29.86
•1.20
3530224
97.50 .00
.84
.000 CFM 9 11.0 IN.HG
.982
DATE 10/29/81
RUN NUMBER 5-6
PROBE LENGTH s TYPE 4* QUARTZ
NUZZLE t I.D. .590
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
PETER BOX NUMBER FBB
PETER HEAD DIFF. 1.91
C FACTOR .94
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
HEFERENCE PRESS. DIFF. .03
READ » RECORD DATA EVERY 10.0 MINUTES
H1
CO
TRAVERSE SAMPLE CLOCK
POINT TIME TIME
NO. (MIN.) (24-HR
' r*i nf *
INIT d
10.0
20.0
30.0
40.0
50.0
60.0 ~
70.0
80.0
90.0
100.0
110. 0
114.8
bk vvn
942"
952
1002
1012
1022
1032
1042
1052
1102
1112
1122
1132
1137
GAS METER
READING
(CU.FT.)
|
1
309.372
314.030
318.710
323.430
328.160
332.940
337.690
342.440
347.200
351.950
356.770
361.630
"'" 363.907
VELOCITY ORIFICE PRESSURE STACK
MEAD DIFFERENTIAL TEPP
(IN.H20) (IN.H20) (OEG.F)
DESIRED
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.44
.44
.44
.44
.44
.44
.44
.44
.44
.44
.44
.44
ACTUAL
.75
.75
.75
.75
.75
.75
.75
.75
.75
.75
.75
.75
DHY GAS METER PUMP SAMPLE
TEMP VACUUM BOX TEMP
(OEG.F) (IN.HG) (OEG.F)
IMPINGER
TEMP
(OEG.F)
I1LET OUTLET
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
49.
52.
57.
60.
63.
65.
66.
67.
68.
69.
70.
71.
47.
48.
50.
51.
53.
55.
56.
57.
58.
59.
61.
63.
3.3
4.7
5.2
5.4
5.7
6.0
7.5
8.3
9.3
9.6
9.8
10.0
629.
604.
598.
610.
617.
620.
618.
618.
620.
620.
619.
623.
38.
36.
3b.
40.
44.
52.
50.
SO.
48.
44.
44.
48.
TOTALS
AVERAGE
114.6
54.535
4.44
.75 520.
63.
55.
7.1 616.
44.
-------
PARTICIPATE FIELD DATA a RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO/HP
TEST
5-6
COKE STACK
TEST DATE
Tb
TF
TT
NP
T
DN
CP
PM
>
1
I-1 VM
00
00
TM
VMSTD
VLC
VHC
BMO
FMD
PC02
P02
PCO
PN2
MO
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OP DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL.* DRY
PERCENT 02 8Y~ VOi;, DRY
PERCENT CO BY VOL.* DRV
PERCENT N2 BY VOL., DRY
MOLECULAR HT-ORY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/29/61
942
1137
110.8
12
.982
.590 IN
. .._••«....
.75 IN-H20
54.535 CU-FT
59.0 F
54.477 SCF
178.8
8.416 SCF
13.38
.866
4.30
11.30
.00
84.40
29.14
27.65
METRIC UNITS
10/29/81
942
1137
114.8
12
.982
15.0 KM
.84
19.1 HM-H2U
1.544 CU-M
15.0 C
1.543 SCf
178.8
.238 SCH
13.38
.866
4.30
11.30
.00
84.40
29.14
27.65
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, AB3.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLO* RATE* DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 PEG Fr 29~.92 iN.HG.
29.66 IN-HG
-1.20 IN-H20
29.77 IN-HG
520. f
20.7 FPS
7466. 30-1N
1796847. 3CFH
3869468.
43.3
.0
ACFH
.0000 GR/03CF*
.000 LB/HR
758.44 *M-HG
-30.48 PH-H20
756.20 *M-HG
271. C
6.3 KPS
4.817 SO-M
50881. SCt'H
109572. ACKH
43.3
.0
.000 f'G/DSCM
.00 KG/HH
00
VO
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NU. 5-6
COKE STACK
VOLUME OF DRV 6AS SAMPLED AT STANDARD CONDITIONS
VMSTD » (17.647 * VM • Y » (PB « PM / 13.6)) / CTM + 460.)
17.647 • 54.535 * .982 * ( 29.86 * .750 / 13.6)
VMSTD * ———————.................—............ = 54.477 OSCF
I 59. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC » .04707 • VLC
VHC * .04707 • "179. * 8.42 SCF
PERCENT MOISTURE IN STACK GAS
BMO • (100. • VHC) / (VMSTD * VHC)
100. * 8.42
BHO * ——————........... 3 13.38 PERCENT
> 54.477 * 8.42
I
M
MD
O
MOLE FRACTION OF DRY STACK GAS
FMO • (100. - BNO) / 100.
ioo. -is.*
FMD * --.——..————.- c .866
100.
AVERAGE MOLECULAR WEIGHT OF DRV STACK GAS
MD * IPC02 • .44) «• (P02 * .32) * (PN2 * PCO) • .28
MD « ( 4.30*44/100) » (11.3*32/100) + t(84.0» .0) * 28/100 = 29.14
MOLECULAR HEIGHT OF STACK GAS
MHS • MD * (1. • IBHO/100)) * 18. * (BHO/100)
MHS a 29.14* (i. -(13.38/100)) 4 18. * (13.38/100) = 27.65
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP • SUM. OF THE SQRT(VH • CT3 t 060.))
VS * 65.49 • CP * OELP / (SQRT(MMS * PS) * PNTS)
VS * 65.49 • .84 • 99.390 / (SQRM 37.65 * 39.77) * 12. : 20.73 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS • AS • 3600/144
OS * 20.73 * f466. 3600/144 B 3669466. ACFM
STACK GAS VOLUMETRIC FLOM AT STANDARD CONDITIONS
OSSTD • 17.647 • 03 * PS * (1. - (BMO/100)) / PERCENT ISOKINETIC
£ ISO • (305.S6*(TS*460.))*U0.002669«VLC)«(VM*Y*(PB+(PM/13.6))/(TM+Q60.)))/(TT*V3*PS*DN*ON)
M
(305.58«( 520.*460.))«((0.002669* 179.)*( 54.535* .9S2*( 29.66*( .750/13.6))/( 59.4460.)))
ISO * ————————————.———.———— — — -—— — ---————.- — . — — ..—-. 9 43.28 PEHCENT
115. • 20.73 • 29.77 * .590 • .590
PARTICIPATE LOADING — CPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN • 15.43 / VMSTD
CS • 0.001 * .0 * 15.43 / 54.477 a .000 GR/DSCF
PARTICIPATE LBS/HR — EPA METHOD 5
PMR * CS • OSSTO / 115.43 • 453.6)
PMR « .000 • 1T96647. / (15.43 • 453.6) * .00
-------
Run No. 5.6
Sample volume =1.54 m3r54.48 scf
Example calculations
CS (Part) =24.9 /I.54 = 16.2 mq/m3
CS (Part) = 0.001 x 24.9 x 15.437 54.48= 0.007 qr/dscf
CS (S02) = 2050/1.54 = 1331 mg/m3
= 1331 x 24.06/64 = 500ppm
= 0.001 x 2050 x 15.43/54.48 = 0.581 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
24.9
0.0
0.0
2050
129
, Concentration,
mg/m
16.2
0.0
0.0
1331
83.8
gr/dscf
0.007
0.0
0.0
0.581
0.036
ppm
500
20
A-192
-------
FIELD DATA
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PAHT/H2S04/S02
OPERATOR BRUFFEY
AMBIENT TEMP. (DEC. F) 75.
BAR. PRESS. (IN.HG) 29.88
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530064
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 5.0 IN.HG
METER CALIB. FACTOR 1.003
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INIT
i
j
>
)
TIME
(MIN.)
o
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80*0
90.0
100.0
110.0
120.0
TIME
(24-HR
1350
1400
1410
1420
1430
1440
1450
1500
1510
1520
1530
1540
1550
READING
(CU.FT.)
930.535
935.270
940.000
944.750
949.450
954.200
958.990
963.750
968.900
973.670
978.430
983.190
988.325
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.060
.050
.050
.050
.060
DIFFERENTIAL
(IN.
DESIRED
.62
.62
.62
.62
.62
.62
.62
.73
.62
.62
.62
.73
H20)
ACTUAL
.62
.62
.62
.62
.62
.62
.62
.73
.62
.62
.62
.73
STACK
TEPP
(OEG.F)
520.
502.
523.
536.
496.
537.
551.
504.
523.
535.
546.
535.
DATE 10/29/81
RUN NUMBER b-i
PHUBE LENGTH ft TYPE 5* HEATED GLASS
NOZZLE : I.U. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER Q
PETER BOX NUMBER FB2
PETEH HEAD OIFF. 1.76
C FACTOR .86
PROBE HtATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. OIFF. .15
DHY GAS METER PUMP SAMPLE IMPINGE*
TEMP
(DEG
INLET
65.
65.
67.
70.
71.
71.
71.
72.
73.
73.
73.
73.
.F)
OUTLET
64.
64.
64.
64.
65.
65.
65.
66.
67.
67.
68.
68.
VACUUM
(IN.HG)
1.5
2.0
2.0
2.5
3.0
3.0
2.5
2.5
2.5
2.5
2.0
3.0
BOX TEMP
(OEG.F)
222.
245.
249.
248.
243.
246.
250.
251.
249.
249.
248.
249.
TEMP
(DEG.F)
49.
52.
53.
54.
52.
SI.
54.
55.
56.
57.
56.
57.
TOTALS
AVERAGE
120.0
57.790
.64
.64 526.
70.
66.
2.4 246.
54.
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
6-1
NO.I COKE BATTERY OUTLET
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
jL VH
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE. DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT I90KINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
« 66 DEC F, 29.92 IN.HG.
39.88 1N-HG
29.79 IN-HG
526. F
17.9 FPS
3Q-IN
SCFH
ACFH
7466.
1529041.
333*937.
114.4
.0
.0000 GR/DSCF*
.000 LB/HN
7b8.95 fM-HG
-30. «8 CM-H20
756.71 PM-HG
274. C
5. a *P3
a. 817 3Q-M
13298. SCFH
no. a
.0
.000 MG/03O
.00 KG/HR
(Ji
-------
vo
CTi
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 6-1
NO.l COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 • VM * V * (PB * PM / 15.6)) / (TM «• 460.)
17.647 • 57.790 • 1.003 * ( 29.88 * .638 / 13.6)
VMSTD « —————————— — — ...... : 57.V81 OSCF
( 68. » 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VNC * .04707 * VLC
VNC » .04707 • 261. » 9.47 SCF
PERCENT MOISTURE IN STACK GAS
BNO • (100. * VNC) / (VM3TD * VNC)
100. * 9.47
BNO * — ————— a 14.04 PERCENT
57.981 » 9.47
MOLE FRACTION OF DRV STACK GAS
FMO « (100. - BNO) / 100.
100. ^ "14.0
FMD * ————————— • .860
100.
AVERAGE MOLECULAR NEieHT OF DRV STACK «s
MD * (PC02 * .44) * (P02 * .32) * (PN2 * PCO) * .28
MO » ( 4.50*44/100) * (10.5*32/100) * ((85.0* .0) * 28/100 = 29.14
MOLECULAR HEIGHT OF STACK GAS
MNS • MD * (1. - (BNO/100)} * 16. * (BNO/100)
MNS * 29.14* (1. -(14.04/100)) * 18. * (14.04/100) * 27.58
-------
STACK CAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SQRTIVH * (TS * 460.))
VS » 85.49 * CP • OELP / (SORT(MHS * PS) * PNTS)
VS * 65.49 * .84 • 85.575 / (SORT( 37.58 * 29.79) * 12. = 17.67 FPS
STACK 6AS VOLUMETRIC FLOH AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS * 17.87 * 7466. 3600/144 > 3334937. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO * 17.647 * OS • PS • (1. - IBMO/100)) / (TS « 460.)
17.647 * 3334937. * 29.79 * (1. - (14.04/100))
OSSTO a ————————............... ..... . = 1529041. SCFH
( 526. * 460.)
PERCENT ISOKINETIC
>
I ISO • (305.58MTS*460.))*l(0.002669*VLC)*(VM*Y*(PB*(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN*ON)
,_,
12 (305.5BM 526.+460.))* ((0.002669"? 2ul.)+( 57.790* 1.003* ( 29.88M .638/13.6))/( 6B.+460.)))
ISO * ————............. ...... .. . . ..... H«.37 PEHCEM
120. * 17.87 * 29.79 * .397 * .397
PARfiCULATE LOADING — EPA METHOD 5 (Af STANDARD CONDITIONS)
CS * 0.001 • MN • 15.43 / VMSTD
CS * 0.001 * .0 * 15.43 / 57.981 • .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR « CS * OSSTD / (IS.43 • 453.6)
PMR « .000 * 1529041. / (15.43 * 453.6) = .00
-------
Run No. 6.1
Sample volume =1.64 m3r57.98 scf
Example calculations
CS (Part) =184.1 / 1.64* 112.2 mq/m3
CS (Part) = 0.001 x 184 x 15.43/57.98 = 0.049 qr/dscf
CS (S02) = 2000/ 1.64=1219.5ma/m3
=1219.5X 24.06/64 = 458ppm
= 0.001 x 2000 x 15.437 57.98 = 0.532 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
184.1
71.0
97.0
2000
24.0
3 Concentration,
mg/m
112.2
43.3
59.2
1219.5
14.6
gr/dscf
0.049
0.019
0.026
0.532
0.006
ppm
458
4
A-198
-------
FIELD DATA
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PART
OPERATOR BRUFFEY
AMBIENT TEMP. (DEG.F) 75.
BAR. PRESS. (IN.HG) 29.88
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBERO) 3530098
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .001 CFM 9 6.0 IN.HG
METER CALIB. FACTOR 1.044
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE
tIME
(MIN.)
CLOCK
TIME
(24-HR
r*i nf* \
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H2U)
ORIFICE PRESSURE
DIFFERENT
(IN.H20)
IAL
STACK
TEKP
(DEG.F)
OESIKEU ACTUAL
INlf
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
135)
1403
1413
1423
1433
1443
1453
1503
1513
1523
1533
1543
1553
151.645
156.000
160.350
164.700
169.050
173.420
177.780
182.130
186.860
191.240
195.590
199.910
204.632
.
.050
.050
.050
.050
.050
.050
.050
.060
.050
.050
.050
•"" .060
.62
.62
.62
.62
.62
.62
.62
.73
.62
.62
.62
.73
.62
.62
.62
.62
.62
.62
.62
.73
.62
.62
.62
.73
520.
515.
528.
541.
525.
543.
555.
515.
524.
538.
522.
538.
DATE 10/29/81
RUN NUMBER t>-2
PHUBE LENGTH 8 TYPE 4' HEATED GLASS
NOZZLE < l.D. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUPHEM 0
PETER BOX NUMBER F10
PETEH HEAD D1FF. 1.80
C FACTOR .86
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. D1FF. .15
DRY GAS METER
TEMP
(DEG.F)
INLET UUTLET
76. 76.
76. 75.
78. ' 76.
80. 76.
81. 77.
81. 76.
81. 76.
81. 76.
81. 76.
81. 76.
79. 76.
79. 75.
PUMP
VACUUM
(IN.HG)
1.0
1.0
2.0
2.5
3.0
3.0
3.5
3.5
3.0
3.0
3.0
4.0
SAMPLE
BOX TEMP
(DEG.F)
248.
266.
264.
264.
265.
255.
257.
254.
258.
256.
251.
255.
IMPINGER
TEMP
(DEG.F)
50.
50.
52.
53.
51.
53.
55.
57.
59.
61.
61.
62.
TOTALS
AVERAGE
120.0
52.987
.64
.64
530.
80.
76.
2.7 258.
56.
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
6-2
NO.l COKE BATTERY OUTLET
TEST
TB
TF
TT
NP
Y
DN
CP
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
ENGLISH UNITS
10/29/81
1353
1553
120.0
12
1.044
.397 IN
.84
METRIC UNITS
10/29/81
1353
1553
120.0
12
1.044
10.1
.84
KM
PM
^ VM
O
p
TM
VMSTD
VLC
VNC
BNO
FMO
PC02
P02
PCO
PN2
MD
MMS
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE CAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGENS AND SILICA GEL,ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL.* DRY
PERCENT 02 BY VOLiT DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRV
MOLECULAR HT-ORY STACK GAS
MOLECULAR NT-STACK GAS
.64 IN-H20
52.987 CU-FT
77.7 F
54.332 SCF
194.4
9.150 SCF
16.2 PM-H20
1.500 CU-M
25.4 C
1.539 SCM
194.4
.259
14.41
.856
4.50
10.50
.00
85.00
29.14
27.53
14.41
.656
4.50
10.50
.00
85.00
29.14
27.53
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
P9 STACK PRES* AB3.
TS AVERAGE STACK TEMP
V3 AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLO* RATE, DRV*
OS ACTUAL STACK FLOM RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 66 DEC F, 29.92 IN.H6.
29.68 IN-HG
"-1.20 IN-H20
29.79 IN-HG
530. F
17.9 FPS
7«b6. SQ-IN
1520006. SCFH
3345471. ACFH
107.B
.0
.0000 GR/OSCF*
.000 LB/HR
758.95 *M-HG
-30.48 PM-H20
756.71 *M-HG
277. C
5.5 KPS
1.817 SQ-M
430fl2. SCt'H
94734. ACHH
107.8
.0
.000 ("G/OSCC
.00 KG/HW
N)
O
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 6-2
NO.l COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.647 » VM * Y • CPB * PM / 13.6)) / (TM * 460.)
17.647 • 52.967 * 1.044 * ( 29.88 » .636 / 13.6)
VMSTD » —— — — ...... 51.332 D3CF
( 78. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC « .04707 • VLC
VMC « .04707 * 194. * 9.15 3CF
PERCENT MOISTURE IN STACK GAS
BMO « (100. • VMC) /~(VMSTD * V«C) ~
•y 100. • 9.15
I BNO * ————.— —. * 14.41 PERCENT
NJ 54.332 * 9.15
Q
fO - - -
MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BMO) / 100.
100. - 1«.4
FMD « ———————— * .856
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MD « (PC02 • .44) « (P02 • .32) * (PN2 * PCO) • .28
MD * ( 4.50*44/100) * (10.5*32/100) * ((85.0* .0) « 28/100 = 29.14
MOLECULAR HEIGHT OF STACK GAS
MMS s MD * (1. • (BMO/100)) + 18. * (BNO/100)
MMS a 29.14* (1. -(14.41/100)) «• 18. •" (14.41/100) s 27.53
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE SQRMVH * (TS » 460.))
V3 * 85.49 * CP • OELP / (SORT(MH3 * PS) * PNTS)
VS * 85.49 • .84 • 85.781 / (SQRT( 27.53 • 29.79) * 12. = 17.92 FPS
STACK 6AS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS * AS • 3600/144
OS • 17.92 • 7466. 3600/144 a 3345471. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTO « 17.647 • OS • PS • (i. • (BNO/tVOD / (TS * 460.)
17.647 • 3345471. • 29.79 • (1. • (14.41/100))
OSSTO « — —— .... . = 1520006. SCFH
( 530. » 460.)
PERCENT ISOKINETIC
ISO * (305.58«(TS+460.))«((0.002669«VLC)»(VM*Y*(PB+(PM/13.6))/(TM+460.m/(TT«V3«PS*DN*DN)
(30S.SB*( 3SO.*460.))*((O.OOZ66W 194.)+( 52.987*1.044*( 29.88+( .638/13.6))/( 78.+460.)))
ISO « — .——.—.— ........... ... ... . i 107.81 PERCENT
120. • 17.92 * 29.79 • .397 * .397
PARTlCULATE LOADING — EPA METHOD 5 (AT~8TANOARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
CS * 0.001 * .0 • 15.43 / 54.332 * .000 GR/DSCF
PARTlCULATE LBS/HR -- EPA METHOD 5
PMR • CS • OSSTD / (15.43 « 453.6)
PMR * .000 * 1520006. / (15.43 * 453.6) = .00
-------
Run No. 6.2
Sample volume = 1.54m r 54.33 scf
Example calculations
CS (Part) =150.8.71.54 =97.9 mq/m3
CS (Part) « 0.001 xl50.8 x 15.43/54.33=0.04.3 qr/dscf
3
CS (S02) = / = mg/m
= x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient .
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
150.8
24.2
0.0
0.0
109.7
4.0
42.3
3 Concentration,
mg/m
97.9
15.7
0.0
0.0
71.2
2.6
27.5
gr/dscf
0.043
0.007
0.0
0.0
0.031
0.001
0.012
ppm
A-204
-------
FIELD OAT*
N)
O
Ul
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 6-3-M8-400
OPERATOR CLARKE
AMBIENT TEMP. (DEC. F) 75.
BAR. PRESS. (IN.HG) 29.88
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 353101
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .001 CFM 8 3.0 IN.HG
METER CALIB. FACTOR .992
READ K RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
1350
1400
1410
1420
1430
1440
1400
1500
1510
1520
1530
1540
1550
EVERY 10.0
GAS METER
READING
(CU.FT.)
671.163
675.675
680.055
684.701
689.000
694.040
698.525
703.200
707.689
712.000
716.520
720.798
725.992
MINUTES
VELOCITY
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.060
.050
.050
.050
.060
ORIFICE
PRESSURE
STACK
DIFFERENTIAL TEMP
(IN.
DESIRED
.62
.62
.62
.62
.62
.62
.62
.72
.62
.62
.62
.72
H20)
ACTUAL
.62
.62
.62
.62
.62
.62
.62
.72
.62
.62
.62
.72
(DEG.F)
520.
502.
523.
537.
547.
537.
553.
553.
523.
535.
499.
530.
DATE 10/29/81
HUN NUMBER 6-3
PROBE LENGTH ft TYPE 5* GLASS HEATED
NOZZLE : I.D. .398
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER
KETER BOX NUKBER FBI
KETER HEAD OIFF. 1.87
C FACTOR .88
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
REFERENCE PRESS. DIFF. 1.50
DHY GAS METER
TEMP
(DEG.F)
INLET OUTLET
74. 70.
74. 69.
70. 68.
80. 67.
00. 69.
81. 69.
81. 69.
82. 70.
82. 70.
82. 70.
82. 71.
81. 70.
PUMP
VACUUM
(IN.HG)
2.0
2.0
2.U
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
SAMPLE
BOX TEMP
(DEG.F)
310.
356.
397.
422.
370.
363.
368.
386.
386.
379.
388.
407.
IMPINGER
TEMP
(DEG.F)
54.
50.
56.
58.
56.
60.
60.
58.
56.
50.
50.
57.
TOTALS
AVERAGE
120.0
54.829
.64
.64 530.
80.
69,
2.0 379.
56,
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
6-3
COKE OVEN OUTLET
I
to
o
cr>
TEST DATE
TB TIME-START
TF TIME-FINISH
TT NET TIME OF TEST, MIN.
NP NET SAMPLING POINTS
Y METER CALIBRATION FACTOR
ON SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL K20 COLLfCTED IN
IMPINGERS AND SILICA GEL,ML,
VMC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BKO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRV GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR MT-DRY STACK GAS
MNS MOLECULAR MT-STACK GAS
ENGLISH UNITS
10/29/81
1550
120.0
12
.992
.396 IN
__ «8a
.64 IN-H20
54.629 CU-FT
74.5 F
53.737 SCF
T75. 4
8.256 SCF
METRIC UNITS
10/29/61
1350
1550
120.0
12
.992
10.1 PM
.84
16.2 MM-H20
1.553 CU-M
23.6 C
1.522 SCP
175.4
.234 SCP
T1VW
.667
4.50
10.50
.00
65.00
29.14
27.66
13.32
.867
4.50
10.50
.00
85.00
29.14
27.66
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
vs AVG STACK" GAS VELOCITY
AS STACK AREA
OSSTD STACK FLON RATE, DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DE6 F, 29.92 IN.H6.
29.ee IN-HG
-1.20 IN-H20
29.79 IN-HG
530. F
17.9 FPS
7«66. SO-IN
1536556. SCFH
3337721.
104.9
.0
ACFH
.0000 GR/OSCF*
.000 LB/HR
750.95 »»M-HG
-30.06 HP-H20
756.71 *M-HG
377. C
5.5 Kpg
0.017 3Q-M
43511. SCHH
94514. ACMH
104.9
.0
.000 t'G/OSCK
.00 KG/HR
I
fO
o
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 6-3
COKE OVEN OUTLET
VOLUME OF ORT GAS SAMPLED AT STANDARD CONDITIONS
VMSTD a (17.64? • VM • Y * (PB + PM / if.6)) / (TM * 460.)
17.647 * 54.629 • .992 * ( 29.86 * .637 / 13.6)
VMSTO » —— ——— —• • = 53.737 OSCF
t 75. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC a .04707 • VLC
V*C a .04707 • 175. i8.26 3CF
PERCENT MOISTURE IN STACK GAS
BMO * (100. * VMC) / (VMSTO » VHC)
. 100. • 8.26
•f BHO » —— —• — r 13.32 PERCENT
ro 53.737 » 8.26
o
oo • —
MOLE FRACTION OF DRY STACK GAS
FMD » (100. - BMO) / 100.
100. - 13.1
FMD • ———————— a ,867
100.
AVERAGE MOLECULAR HEIGHT OF DRV STACK 6T3
MD * (PC02 • .44) * (P02 * .32) + (PN2 4 PCO) * .28
MO « ( 4.50*44/100) •» (10.5*32/100) » ((85.0+ .0) * 28/100 = 29.14
MOLECULAR HEIGHT OF STACK GAS
MRS a MD * (1. • (BHO/100)) » 18. • (BHO/100)
MRS * 29.14* (1. -(13.32/100)) t 18. * (13.32/100) = 27.66
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE SORT(VH * (TS * 460.))
VS « B5.49 • CP • OELP / (SQRT(M«S * PS) • PNT3)
VS « 85.49 * .04 • 95.778 / (SORT( 27.66 * 29.79) • 12. = 17.68 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS > VS * AS * 3600/144
OS « 17.88 • 7466. 3600/144 * 3337721. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO « 17.647 • OS * PS • (1. - (BMO/100J) / (TS « 460.)
17.647 * 3337721. * 29.79 • (1. - (13.32/100))
OSSTO « ———————— — s 153b55b. SCFH
( 530. » 460.)
", PERCENT ISOKINETIC
K>
O ISO » (305.58*(TS*460.))*((0.002669*VLC)*(VM*Y*(PB*(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN*ON)
VD
(305.58*( 530.V460.))*((6.002669* 175.)»{ 54.829* ,992*( 24.8B«( .637/13.6))/( 75.+460.)))
ISO » -i——.———————.......................—............. —.............................. * 104.95 PERCEM
120. * 17.88 • 29.79 * .398 * .398
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS a 0.001 * MN • 15.43 / VM3TD
CS * 0.001 * .0 • 15.43 / 53.737 * .000 GR/DSCF
PARTICIPATE LBS/HR — EPA METHOD 5
PMR * CS * OSSTO / (15.43 * 453.6)
PMR • .000 • 15)6556. / (15.43 i~453.6) = .00
-------
Run No. 6.3
3
Sample volume = 1 .52 m r 53.74 scf
Example calculations
CS (Part) = 34.3/1.52 = 22.6 mq/m3
CS (Part) = 0.001 x 34-3 x 15.437 53.74= 0.010 qr/dscf
CS (S02) =1900 /1.52 . 1250mg/m3
J250
0.001 x 190° x 15.43/53.74 = 0.546 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
34.3
2.8
3.8
1900
97.6
o Concentration,
mg/m
22.6
1.8
2.5
1250
64.2
gr/dscf
0.010
0.0008
0.001
0.546
0.028
ppm
470
16
A-210
-------
FIELD DATA
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 6-4-M5-400
OPERATOR CLARKE
AMBIENT TEMP. (DEG.F) 75.
BAR. PRESS. (IN.HG) 29.00
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530003
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .04
THERM. NO.
LEAKAGE .120 CFM 3 c.O IN.HG
METER CALI8. FACTOR 1.016
READ * RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT TIME
NO. (MIN.)
INlt 0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
00.0
90.0
100.0
110.0
120.0"
TIME
(24-HR
1354
1404
1414
1424
1434
1444
1454
1504
1514
1524
1534
1544
1554
READING
(CU.FT.)
00.937
93.212
97.425
101.926
106.210
110.736
115.426
119.660
124.111
120.140
132.670
137.220
142.007
HEAD
(IN.H20)
•
.050
.050
.050
.050
.050
.050
.050
.060
.050
.050
.050
.060
DIFFERENTIAL
(IN.
DESIRED
.62
.62
.62
.62
.62
.62
.62
.72
.62
.62
.62
.72
H20)
ACTUAL
.62
.62
.62
.62
.62
.62
.62
.72
.62
.62
.62
.72
STACK
TEMP
(DEG.F)
550.
515.
526.
541.
519.
537.
556.
514.
524.
535.
523.
539.
DATE 10/29/81
RUN NUMBER 6-4
PROBE LENGTH « TYPE 6 FT GLASS HEATtD
NOZZLE 1 1.0. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER
METER BOX NUMBER FB5
METER HEAD DIFF. 1.86
C FACTOR .88
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
REFERENCE PRESS. DIFF. 1.50
DRY GAS METER PUMP SAMPLE IMPINGEH
TEMP VACUUM
(DEG
INLET
04.
05.
08.
90.
92.
94.
94.
94.
94.
93.
92.
92.
.F) (IN.HG)
OUTLET
02.
02.
63.
65.
06.
66.
00.
60.
88.
88.
67.
87.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(DEG.F)
370.
401.
434.
442.
395.
403.
406.
411.
399.
390.
407.
421.
TEMP
(OEG.M
46.
44.
42.
40.
52.
50.
40.
46.
44.
42.
44.
42.
TOTALS
AVERAGE
120.0
46.702
.64
.64 532.
91,
66.
1.0 407.
46.
-------
PARTICIPATE FIELD DATA a RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
6-4
COKE OVEN OUTLET
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
1
10 VM
NJ
TM
VMSTD
VLC
VNC
BMO
FMD
PC02
P02
PCO
PN2
MO
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRV
PERCENT N2 BY VOL., DRY
MOLECULAR MT-ORY STACK GAS
MOLECULAR MT-STACK GAS
ENGLISH UNITS
10/29/61
1354
1554
120.0
»z
1.016
.397 IN
.64
.64 IN-H20
46.702 CU-FT
88.5 F
45.666 SCF
179.5
8.449 SCF
"15.61
.644
4.50
"iO.50
.00
85.00
-?9.14
27.40
METRIC UNITS
10/29/81
1354
1554
120.0
12
1.016
10.1
.64
16.2
1.322
31.4
1.294
179.5
.239
15.61
.844
4.50
10. SO
.00
85.00
29.14
27.40
KM
PM-H20
CU-M
c
sen-
SCM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRE3 OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLON RATEr DRY*
US ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 66 DEC F, 29.92 1N.H6.
29.68 IN-HG
-1.20 IN-H20
29.79 IN-HG
532. F
18.0 FPS
7466. SO-IN
1500961. 3CFH
758.95 *M-HG
-30.ae MM-H20
756.71 HM-MG
C
5.5 t'PS
0.817 SO-M
3356748
91
ACFH
.8
.0
.0000 GR/DSCF*
.000 LB/HR
95053.
91.8
.0
.000
.00
ACHH
CG/OSCK
KG/HH
NJ
M
U>
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 6-4
COKE OVEN OUTLET
VOLUME OF DRV 6AS SAMPLED AT STANDARD CONDITIONS
VMSTO « (17.647 • VM • Y * (PB * PM / 13.6)) / (TM «• 460.)
17.647 • 46.702 • 1.016 * ( 29.68 * .637 / 13.6)
VMSTD * ——————................... .............— - 45.686 DSCF
( 89. » 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC * .04707 * VLC
VHC « .04707 • 160. » 8.45 SCF
PERCENT MOISTURE IN STACK GAS
BHO « (100. • VHC) / (VMSTD * VHC)
100. • 8.45
BHO » ———.—.. ...... c 15.61 PERCENT
45.686 » 8.45
*» """ —. ...
MOLE FRACTION OF DRV STACK GAS
FMO • (100. - BHO) / 100.
100. -"15.6
FMO * —————— 9 .844
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK CAS
MD * (PC02 • .44) * (P02 * .32) * (PN2 * PCO) * .28
MD a ( 4.50*44/100) » (10.5*32/100) + ((85.0* .0) * 28/100 > 29.14
MOLECULAR HEIGHT OF STACK GAS
MHS • MD • (1. - (BHO/100)) «• 18. * (BHO/100)
MHS • 29.14* (1. -(IS.61/100)) + 16. « (15.61/100) s 27.40
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SORT(VH * (TS * 460.))
VS * 85.49 * CP * DELP / (SORT(MWS • PS) • PNTS)
VS * 85.49 • .84 * 85.862 / (SORT( 27.40 * 29.79) * 12. = 17.96 FP3
STACK 6AS VOLUMETRIC FLOH AT STACK CONDITIONS
OS « VS • AS * 3600/144
OS » 17.98 • " f466. 3600/144 a 3356708. ACFH
STACK 6AS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO « 17.647 i'OS * PS • (t. • (BNO/tfO)) / (TS * 460.)
17.647 • 3356748. • 29.79 * (1. - (15.61/100))
OSSTD s ———-—.———.———.—-———— — — s 1500961. SCFH
f 532. » 460.)
PERCENT ISOKINETIC
ISO « (305.58«(TS*460.))«((0.002669«VLC)*(VM«T*(PB»(PM/13.6))/(TM*460.)))/(TT«>VS«PS*DN*ON)
(305.58«( 552.»460.))«((0.002669* 180.)»( 46.70Z*!.016*( 29.8B*( .637/13.6))/( 89.•460.)))
ISO » —————— — ..... ...... .... ....... ...... * 91.80 PEHCENT
120. • 17.98 • 29.79 * .397 • .397
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 • MN * 15.43 / VMSTD
CS « 0.001 * .0 * 15.43 / 45.686 « .000 6R/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR « CS * OSSTD / (15.43 * 453.6)
PMR » .000 * 1500961. / (IS.43 * 453.6) = .00
-------
Run No. 6.4
Sample volume =1.29 m3.45.69 scf
Example calculations
CS (Part) = 26.9/1.29 = 20.8 ma/m3
CS (Part) = 0.001 x26.9 x 15.43/45.69 = O.Q09 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
26.9
0.0
0.0
118.3
5.9
154.0
3 Concentration,
mg/m
20.8
0.0
0.0
91.7
4.6
119.4
gr/dscf
0.009
0.0
0.0
0.040
0.002
0.052
ppm
A-216
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BAR.PRESS.(IN.H6)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
COKE STACK
METHOD 5-250
DO-MP
61.
29.88
.00
97.50
.80
.00
.016 CFM 8 10.0 IN.HG
1.033
DATE 10/29/81
RUN NUMBER 6-5
PROBE LENGTH ft TYPE 6* GLASS
NUZZLE > l.D. .374
ASSUMED MOISTURE 11.0
SAMPLE BOX NUPBER
HETER BOX NUMBER FB4
PETER HEAD DIFF. i.ae
C FACTOR .92
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .18
READ ft RECORD DATA EVERY 10.0 MINUTES
>
TRAVERSE SAMPLE CLOCK
POINT TIME TIME
NO. (MIN.) (24-HR
1*1 nrw %
INtt ~ 0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100. 0
110.0
120.0
tub VV" /
1353"
1403
1413
1423
1433
1443
1453
1503
1513
1523
1533
1543
i553
GAS METER
READING
(CU.FT.)
VELOCITY ORIFICE PRESSURE
HEAD DIFFERENTIAL
(IN.H20) (IN.H20)
DESIRED
909.697
914.440
919.130
923.810
928.440
933.160
937.860
942.550
947.240
951.910
956.610
961.300
965.996
.070
.070
.070
.070
.070
" .070
.070
.070
.070
.070
.070
" .070
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
ACTUAL
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
STACK
TEPP
(DEG.F)
ONY GAS METER PUMP SAMPLE
TEMP VACUUM BOX TEMP
(OEG.F) (IN.HG) (DEG.F)
1MPINGEH
TEMP
(OEG.F)
INLET OUTLET
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
64.
65.
67.
69.
70.
71.
72.
72.
72.
72.
72.
72.
64.
64.
63.
64.
65.
65.
66.
66.
66.
67.
67.
67.
8.4
8.7
8.7
8.7
8.6
8.7
8.7
8.7
8.7
8.7
8.7
8.8
225.
253.
249.
247.
240.
245.
248.
251.
251.
251.
247.
246.
45.
44.
4
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO-MP
TEST
6-5
COKE STACK
I
00
ENGLISH UNITS
TEST
TB
TF
TT
NP
V
DN
CP
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
10/29/81
1553
1553
120
12
1
.0
.033
.374 IN
.84
METRIC UNITS
10/29/81
1353
1553
120
12
1
9
.0
.033
.5
.84
CM
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VHC VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR MT-OftV STACK GAS
MMS MOLECULAR NT-STACK GAS
.72 IN-H20
56.299 CU-FT
67.6 F
58.228 SCF
213.8
10.064 SCF
18.3 CM-H20
1.594 CU-M
19.8 C
1.649 SCC
213.8
.285 SCC
14.74
.853
4.50
10.50
.00
85.00
29.14
27.50
14
4
10
85
29
27
.74
.853
.50
.50
.00
.00
.14
.50
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE, DRY*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 29.92 IN.H6.
29.68 IN-HG
.00 IN-H20
29.88 IN-HG
520. F
20.7 FPS
7466. SO-IN
1776813. SCFH
3873037.
111.4
.0
ACFH
.0000 GR/OSCF*
.000 LB/HH
758.95 CM-HG
.00 MM-H20
758.95 KM-HG
271. C
6.3 CP3
4.817 SQ-M
50314. SCHH
109673. ACI'H
111.4
.0
.000 PG/OSCP
.00 KG/HR
to
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 6-5
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.647 * VM * Y * (PB » PM / 15.6)) / (TM * 460.)
17.647 • 56.299 • 1.033 * ( 29.88 » .720 / 13.6)
VMSTO « ..————.................................—..... = 58.228 DSCF
( 66. » 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC * .04707 * VLC
VMC « .04707 • 214. I T6.06 SCF
PERCENT MOISTURE IN STACK GAS
BMO « (166. * VMC) / (VMSTD «• VMC) "™~
> 100. * 10.06
I BMO a .———.— .......... s 14.74 PERCENT
^ 58.228 * 10.06
N)
O ...... . .
MOLE FRACTION OF DRV STACK GAS
FMO • (100. - BMO) / 100.
100. • 14.7
FMD « ————.——.—. * .853
100.
AVERAGE MOLECULAR HEIGHT or DRY STACK ns
MD « (PC02 * .44) + (P02 « .32) * (PN2 * PCO) * .28
MO • ( 4.50*44/100) «• (10.5*32/100) * ((85.0* .0) • 28/100 = 29.14
MOLECULAR HEIGHT OF STACK GAS
MMS • MD • (1. • (BMO/IOO)) + 18. • (BNO/100)
MMS « 29.14* (1. -(14.74/100)) » 18. *"T14.74/100) « 27.50
-------
>
STACK 6*3 VELOCITY AT STACK CONDITIONS
OELP * SUM. OF THE SQRT(VH * (TS * 460.))
VS * 65.49 * CP • OELP / (SORT(MW3 * PS) • PNTS)
VS » 85.49 • .84 • 99.390 / (30RT( 37.50 • 29.88) * 12. = 20.75 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
03 » VS * AS * 3600/144
OS « 20.75 * 7466. 3600/144 « 3873037. ACFH
STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTD • 17.647 * OS • PS * (1. • (BNO/100)) / (TS » 460.)
17.647 * 3873037. • 29.88 * (1. - (14.74/100))
03STD • ———————————————— ---- — * 1776813. SCFH
( 520. «• 460.)
__. . . „_
PERCENT ISOKINETIC
130 • (305.58«(T3*460.))«((0.002669«VLC)+(VM«Y*(PB«(PM/13.6))/(TM+460.)))/(TT«V3*P3«DN«ON)
(30S.§8*( 520. +460.))*((d. 002669* 214. )»( 56. 299*1. 033«( 29. 88«( .720/13.6) )/( 68.4460.)))
ISO « — — ..... ...... ..... --- ........... --- ...... ------------ .... . ------- . --- ...... --- ... ---------- . a 111.37 PERCENT
120. • 20.75 * 29.88 * .374 * .374
PARTICULATE LOADING— EPA METHOD 5 (AT "STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
C3 » 0.001 * .0 * 15.43 / 58.228 « .000 GR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR * CS • OS3TD / (15.43 • 453.6)
PMR « .000 • 1776813. / (15.43 • 953.6) r .00
-------
Run No. 6.5
o
Sample volume = 1.65 m ,58.23 scf
Example calculations
CS (Part) =195.7/1.65 = 118.6 mq/m3
CS (Part) = 0.001 x!95.7 x 15.43/58.23 = 0.052 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sul f uric acid mist
As H2$04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
195.7
42.3
37.6
33.2
30.3
25.8
0.0
0.0
20.0
6.4
15.2
2 Concentration,
mg/m
118.6
25.6
22.8
20.1
18.4
15.6
0.0
0.0
12.1
3.9
9.2
gr/dscf
0.052
0.011
0.010
0.009
0.008
0.007
0.0
0.0
0.005
0.002
0.004
ppm
1
A-222
-------
FIELD DATA
PLANT . REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE STACK
SAMPLE TYPE METHOD 8-600
OPERATOR DO/MP
AMBIENT TEMP. (DEC. FJ 61.
BAR. PRESS. CIN.H6) 29. S8
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER (3) 3530209
STACK INSIDE DIN. (IN) 97.50 .00,
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFN 8 7.0 IN
METER CALIB. FACTOR .982
READ ft RECORD DATA EVERT 10. 0 MINUTES
,HG
TRAVERSE SAMPLE CLOCK CAS METER VELOCITY ORIFICE PRESSURE
POINT TIME TIME READING HEAD DIFFERENTIAL
NO. (MIN.) (24-HR (CU.FT.) (IN.H20) (IN.H20)
STACK
TEMP
(OEG.F)
DESIRED ACTUAL
INIT 0 1392 364. 163
10.0 1402 368.920 .070
> 20.0 1412 373.660 .070
' 30.0 1422 378.370 .070
isj 40.0 1432 383.050 .070
U> SO.O 1442 387.780 .070
60.0 1452 392.500 .070
70.0 1502 397.230 .070
BO.O 1512 401.960 .070
90.0 1522 406.690 .070
100.0 1532 411.420 .070
110.0 1542 416.150 .070
120.0 1552 420.865 .070
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
.32 .75
920.
520.
520.
520.
520.
•520.
520.
520.
920.
520.
520.
920.
DATE 10/29/81
RUN NUMBER 6-6
PROBE LENGTH ft TYPE 4* QUARTZ
NOZZLE I I.D. .620
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBER FBS
METER MEAD OIFF. 1.91
c FACTOR .92
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .02
DRV GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM BOX TEMP TEMP
(DE6.F) (IN.HG) (DEG.F) (DE6.F)
INLET OUTLET
61. 60. .6 SB6. 38.
62. 60. .7 582. 36.
65. 60. 7 509. 36.
68. 61. 9 542. 40.
70. 62. 0 545. 38.
72. 63. 3 583. 38.
72. 63. 4 584. 40.
73. 64. 7 594. 40.
73. 65. 8 587. 38.
73. 65. 9 601. 38.
73. 65. 1 599. 38.
73. 65. 5 600. 40.
TOTALS
AVERAGE
120.0
56.702
9.32
.75 520.
70.
63.
4.5 576,
38.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO/HP
TEST
6-6
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
1
N> VM
NJ
TM
VMSTO
VLC
VMC
UNO
FMD
PC02
P02
PCO
PN2
" MO
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL M20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE 8V VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL.* ORV
PERCENT CO BY VOL.* DRV
PERCENT N2 BY VOL., DRV
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/29/81
1352
1552
120.0
12
.982
.620 IN
.84
.75 IN-H20
56.702 CU-FT
66.2 F
55.903 9CF
101.7
9.494 SCF
_li.S2
.855
4.50
10.50
.00
85.00
29.14
27.52
METRIC UNITS
10/29/81
1352
1552
120.0
12
.982
15.7 MM
.64
19.1 IMM-H20
1.606 CU-M
19.0 C
1.583 SCH
201.7
.269 SCN
14.52
.855
4.50
10.50
.00
85.00
29.14
27.52
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES Of STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
QSSTD STACK FLOW RATE* DRV*
OS ACTUAL STACK FLO* RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
C3 FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 010?; 89.94 IN.MG.
29.OS IN-HG
•1.20 IN-M20
29.74 IN-MG
920. F
20.8 FPS
7466. SO-IN
17779S5. SCFH
3877090. ACFH
38.9
.0
.0000 GR/OSCF*
.000 L8SHR
758.99 MM-HG
•30.08 MM-H80
75*.71 MM-HG
271. C
6.3 MP8
4.817 80-M
S0346. 8CMH
109786. ACMH
38.9
.0
.000 M6/DSCH
.00 KS/HR
ro
to
ui
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 6-6
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.647 * VM * Y * (Pft 4 PM / IS. 6)) / (TM » 460.)
17.647 * 56.702 * .982 • ( 29.88 « .750 / 13.6)
VMSTD • — — — -— ........................ ........ ........ . 53.903 OSCF
( 66. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 • VLC
VMC • .04707 * 202. « 9.49 SCr
PERCENT MOISTURE IN STACK CAS
0MO i (100. • VKC7 / (VHSTO » VHC)
^ 100. • 9.49
•f BWO » ——.—.—.- ............. :» 14.51 PERCENT
to 55.903 * 9.49
•-OV-
MOLE FRACTION OF DRY STACK GAS
FMO • (100. - BMO) / 100.
- loft. • 14.S
FMD • — — — — ............. • .855
100.
AVERAGE MOLECULAR "EIGHT OF DRV STACK GAS
MO • (PC02 * .44) » (P02 * .32) * (PN2 • PCO) « .28
MO a ( 4.50*44/100) * (10.5*32/100) * ((85.0* .0) * 28/100 • 29.14
MOLECULAR HEIGHT OF STACK GAS
MHS a MO • (1. • (BNO/100)) * 18. • (BNO/100)
MNS a 89.14* (1. -(14.52/100)) * 18. • (14.52/100) a 27.52
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE 90RTCVM • (TS » 460.))
VS • 65.49 • CP • OELP / (SQRT(MMS • PS) • PUTS)
VS « B5.49 * .04 • 99.390 / (80RT( 27.92 • 29.79) • 12. • 20.77 PPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
03 • VS • AS • 3600/144
OS • 20.77 • 7466. 3600/144 • 3877090. ACFM
STACK CAS VOLUMETRIC FLOH AT STANDARD CONDITIONS
OSStO • if.647 • OS • PS~* Tl. • (MO/100)) / (T8 * 460.)
17.647 • 3877050. * 29.79 • (1, - (14.92/100))
OSSTO • ——————.................................... • 17779S3. SCFM
( 920. » 460.)
PERCENT I80KINETIC
>
I ISO » (309.58*(TS»460.))*((0.002669*VLC)»(VM*Y*(PB*(PM/13.6))/(TM*460,)))/(TT*VS«PS*DN*ON)
to
^ (36S.5M( S20.+460.))»((0.002669* 202.)+( 56.702* .*82*( 29.88«( .750/13.6))/( 66.«460.)))
ISO » .——..—.————.—[[[ . 38.88 PERCENT
120. • 20.77 • 29.79 * .620 • .620
PARTlCULAte LOADING —EPA METHOD 9 (AT STANDARD CONDITIONS)
CS » 0.001 * MN • 19.43 / VMSTD
CS * 0.001 * .0 • 19.43 / 99.903 • .000 6R/D8CF
PARTICULATE LBS/HR — EPA METHOD 9
-------
Run No. 6.6
Sample volume =1.58 m3T 55.90 scf
Example calculations
CS (Part) =30.9 /.58 =19.6 ma/m3
CS (Part) = 0.001 x30.9 x 15.43/55.90= 0.008 gr/dscf
3
CS (S02) =2010/1.58=1272 ma/m
= 1272 x 24.06/G4 =478 ppm
= 0.001 x2010 x 1 5. 43/.55JiP
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
30.9
0.0
0.0
2010
115
3 Concentration,
mg/m
19.6
0.0
0.0
1272
72.8
gr/dscf
0.008
0.0
0.0
0.555
0.032
ppm
478
18
A-228
-------
FIELD DAT*
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PART/H2S04/S02
OPERATOR BRUFFEY
AMBIENT TEMP. (DEC. F) 54.
BAR. PRESS. (IN. HO) 29.92
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530043
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 8 5.0 IN.MG
METER CALIB. FACTOR 1.003
READ » RECORD DATA EVERY 10. 0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT TIME
NO. (MIN.
INIT 0
10.0
20.0
> 30.0
to 40.0
to 50.0
vo 60.0
70.0
80.0
90.0
100.0
110.0
120.0
TIME
) (24-HR
930
940
950
1000
1010
1020
1030
1040
1050
1100
1110
1120
" 1130
READING
(CU.FT.)
988.550
993.730
998.590
3.600
9.050
13.680
18.350
23.840
28.590
33.300
39.130
43.820
48.499
HEAD
(IN.H20)
.060
.060
.060
.070
.050
.050
.070
.050
.050
.080
.050
".050
DIFFERENTIAL
(IN.
DESIRED
.73
.73
.73
.87
.62
.62
.87
.62
.62
1.00
.62
.62
H20)
ACTUAL
.73
.73
.73
.87
.62
.62
.87
.62
.62
1.00
.62
.62
STACK
TEMP
(OEG.F)
t
316.
536.
550.
503.
514.
540.
523.
565.
562.
505.
516.
527.
DATE 10/30/81
RUN NUMBER 7-1
PROBE LENGTH • TYPE 6* HEATED GLASS
NOZZLE 1 I.D. .398
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER o
METER BOX NUMBER FB2
METER HEAD OIFF. i.76
C FACTOR .86
PROBE HEATER SETTING 250.
MEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .is
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP
(DEG.F)
INLET
55.
56.
60.
63.
66.
67.
69.
70.
70.
70.
71.
71.
OUTLET
.54.
54.
54.
55.
57.
•58.
60.
61.
62.
63.
63.
64.
VACUUM
(IN.HG)
1.5
1.5
1.5
2.0
2.5
2.5
2.5
2.5
2.5
3.0
3.5
3.5
BOX TEMP
(DEG.F)
240.
247.
292.
254.
258.
257.
254.
256.
249.
244.
252.
255.
TEMP
(DEG.F)
46.
44.
46.
46.
47.
49.
56.
59.
60.
57.
•35.
93.
TOTALS
AVERAGE
120.0
59.949
.72
.72 530.
66.
59.
2.4 292.
52.
-------
PARTICIPATE FIELD DATA a RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
7-1
NO.I COKE BATTERY OUTLET
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
E V"
OJ — _..
0
TM
VMSTD
vie
•VHC
Slid
FMD
PC02
P02
PCO
PN2
MO
MM 3
TIME-START
TIME-FINISH
NET TIME OF TEST* MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAB SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL M20 COLLECTED IN
IMPINGERS AND SILICA GEL*ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BY VOL.* DRV
PERCENT 62 BY VOL.* DRY
PERCENT CO BY VOL.* DRV
PERCENT N2 BY VOL.* DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/30/81
930
1130
120.0
12
1.003
.398 IN
.84
.72 IN-H20
59.949 CU-FT
62.2 F
60.903 SCF
1*2.1
4.042 SCF
12.43
.871
4.00
11.00
, .00
85.00
29.08
27.65
METRIC UNITS
10/30/81
430
1130
120.0
12
1.003
10.1 MM
.84
18.3 MM-H20
1.648 CU-M
16.8 C
1.725 SCM
142.1
.256 SCM
12.43
.871
4.00
11.00
.00
85.00
24.08
27.65
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRE8 OF STACK 6AS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK QAS VELOCITY
AS STACK AREA
QSSTD STACK FLOW RATE* DRT«
OS ACTUAL STACK FLO* RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 DEC FV 29.91 IN.HG.
29.92 IN-MG
-1.20 IK-M20
29.03 IN-HG
530. F
1ft.9 FPS
7466. SO-IN
1636079. SCFM
3SS26SS.
111.7
.0
ACFH
.0000 GR/DSCF*
.000 LB/MR
759.97 MM-H6
•30.4ft MM*N20
757.73 MM-HG
277. C
5.ft HPS
•.617 SO*M
46329. SCMH
100034. ACMH
111.7
.0
.000 N6/OSCK
.00 KG/HR
to
U)
-------
EXAMPLE PARTICULAR CALCULATIONS TEST NO. 7-1
NO.l COKE BATTERY OUTLET
VOLUME OF OUT 6AS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 *~ VM * Y * (PB * PM / 13.6)) / (TM » 460.)
17.647 • 39.949 * 1.003 • ( 29.92 «• .721 / IS. 6)
VMSTD • ——————————————————— • 60.903 03CF
( 62. » 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 • VLC
VNC • .04707 • 192. • 9.04
PERCENT MOISTURE IN STACK 6AS
BNO » (iOOi~* VHC) / (VMSTO * VWC)
100. * 9.04
BMO • .——.———.——— « 12.93 PERCENT
^ 60.903 * 9.04
I
to
CO
M MOLE FRACTION OF DRY STACK CAS
FMO » (100. » BNO) / 100.
100. - 12.9
FMD • •...—•....••-•••.»•«•. • .$71
100.
AVERAGE MOLtCULA* HEIGHT OF DRY STACK CAS
MO • (PC02 * .44) * (P08 • .32) * (PN2 * PCO) * .26
MO • ( 4.00*44/100) » (11.0*32/100) * ((6S.O* .0) • 28/100 • 29. OS
MOLECULAR NEI6MT OF STACK GAS
MHS » MD • (1. • (BNO/100)) » IS. * (BNO/100)
MHS » 29.06* (i. -(12.93/100)) » 18. * (12.93/100) • 27.65
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. Of THE SQRT(VH * (TS + 4*0.))
VS • 85.49 • CP • DELP / (SQRT(MMS * PS) • PNTS)
VS • 8b.«9 * .84 • 90.827 / (SQRT( 27.65 • 29.83) • 12. • 18.93 FPS
STACK CAS VOLUMETRIC FLOM AT STACK CONDITIONS
OS * VS • AS * 3*00/144
OS « 18.93 • 7466. 3600/144 • 3531(35. ACFH
STACK 6AS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD « 17.647 * Q3 • M • (1. - (BNO/100H / (T8 * 460.)
17.647 • 3532635. * 29.83 • (1. • (12.93/100))
OSSTD » — ———-.———— .............. .... ...........* 1636079. 3CFH
( 530. » 460.)
> PERCENT ISOK1NETIC
I
ISO • (305.58«(TS*460.))*((0.002669*VLC)«(VM«Y*(PB«(f>M/13.6))/(TM«460.)))/(TT*V8*P
-------
Run No. 7-1
Sample volume =
Example calculations
, 60.90 scf
CS (Part) =195. 8/ 1.73L 113.2mq/m3
CS (Part) = 0.001 x195-8 x 15.43/60.90= 0.050 qr/dscf
CS (S02) = _ / _ = _ mg/m3
= _ x 24. 06/ _ = _ ppm
= 0.001 x _ x 15.43/ _ = _ gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
195.8
3 Concentration,
mg/m
113.2
gr/dscf
0.050
ppm
A-234
-------
FIELD DATA
ro
10
uv
PLANT REPUBLIC 8TEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PART
OPERATOR BRUFFEY
~ AMBIENT TEMP. (OEG.F) 54.
BAR. PRESS. (IN. HG) 29.93
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530066
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 8 6.0 IN.H6
METER CALIB. FACTOR 1.044
READ ft RECORD DATA EVERY 10. 0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INlf
TIME
(MIN.)
a
10.0
20.0
30.0
40.0
SO.O
60.0
70.0
80.0
90.0
100.0
110.0
120.0
TIME
(24-HR
933
943
953
1003
1013
1023
1033
1043
1053
1103
1113
1123
1133
READING
(CU.FT.)
204.803
209.480
214.180
216.880
223.930
228.290
232.670
237.720
242.080
246.450
251.890
256.250
260.606
HEAD
(IN.H20)
.060
.060
.060
.070
.050
.050
.070
.050
.050
.080
.050
.050
DIFFERENTIAL
(IN.
DESIRED
.73
.73
.73
.87
.62
.62
.87
.62
.62
1.00
.62
.62
H20)
ACTUAL
.73
.73
.73
.87
.62
.62
.87
.62
.62
1.00
.62
.62
STACK
TEMP
(OEG.F)
328.
541.
557.
504.
528.
349.
547.
565.
563.
507.
518.
333.
DATE 10/30/81
RUN NUMBER 7-2
PROBE LENGTH ft TYPE 5* HEATED GLASS
NOZZLE t I.D. .377
ASSUMED MOISTURE 12.0
8AMPLE BOX NUMBER 0
METER BOX NUMBER FIO
METER HEAD DIFF. 1.80
C FACTOR .86
PROBE HEATER SETTING 850.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .15
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP
(OEG.F)
INLET
58.
60.
64.
67.
70.
71.
72.
73.
74.
74.
75.
76.
OUTLET
58.
58.
60.
61.
61.
63.
64.
66.
66.
67.
68.
69.
VACUUM
(IN.HG)
1.
1.
2.
2.
2.
2.
3.0
2.5
3.0
3.0
3.0
3.0
BOX TEMP
(DE6.F)
259.
266.
264.
262.
264.
259.
258.
258.
253.
246.
253.
258.
TEMP
(OEG.F)
•2.
44.
46.
43.
47.
•49.
54.
39.
62.
56.
35.
32.
TOTALS
AVERAGE
120.0
55.803
.72
.78 537.
70.
63.
2.5 258.
31.
-------
PARTICIPATE FIELD DATA I RESULTS TABULATION
i
PLANT* NAME AND ADDRESS . TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND , BRUFFEY
TEST
T-Z
NO.l COKE BATTERY OUTLET
>
NJ
to
cn .
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
VM
TM
VMSTO
flME-lfART
TIME-FINISH
NET TIME OF TEST, MlN.
NET SAMPLIN9 POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV 6AS SAMPLED
AT METER CONDITIONS
AVERA6E GAS METER TEMP
VOLUME OF DRV 6AS SAMPLED
ENGLISH UNITS
10/30/61
«1
1133
120.0
12
1.044
.377 IN
.._.. •**
.72 IN-H20
55.803 CU-FT
66.5 F
98. 552 SCF
METRIC UNITS
10/30/81
933
1133
120.0
12
1.044
9.6 KM
.84
18.3 MM-H20
1.580 CU-M
19.1 C
1.658 SCM
AT STANDARD CONDITIONS*
VLC TOTAL M20 COLLECTED IN
IMPINBERS AND SILICA GELtML.
VNC VOLUME OF WATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRV 6AS
PC02 PERCENT C02 BV VOL.* DRV
pol PERCENT 02 BY VOL.* 0*v
PCO PERCENT CO BV VOL.. DRV
PN3 PERCENT N2 BV VOL., ORV
MO MOLECULAR NT-DRY STACK GAS
MKS MOLECULAR NT-STACK GAS
HI. a
8.557 SCF
101.8
.242 SCM
12.75
.872
4.00
11.00
.00
85.00
29.08
27.67
12.75
.872
4.00
11.00
.00
85.00
29.08
27.67
-------
PB BAROMETRIC PRESSURE
P3I STATIC PRES OP STACK 6AS
PS STACK PRES, ABS.
TS AVEMA6E STACK TEMP
VS AV6 STACK 6A9 VELOCITY
AS STACK AREA
QSSTD STACK FLON RATE* DRV*
03 ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 3
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 68 DES F, 29.W IN.H6.
29
-1
29
537
19
7466
•
•
.
•
•
•
93
20
64
0
IN-HG
IN-H20
IN-HG
F
PPS
80-IN
1633313.
3543545
•
SCFH
ACFH
119.9
760
•30
757
280
5
4
46251
100343
119
.0
•
•
0000
000
GR/DSCF*
LB/HR
.22
.46
.98
•
.•
.817
•
•
.9
.0
.000
.00
•MM-H6
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 7-2
NO.l COKE BATTERY OUTLET
VOLUME Of DRY GAS SAMPLED AT STANDARD CONDITIONS
VM3T6 • (i?.*«7 • VM • Y * IPB * PM / IS.*)) / (TM * 460.)
17.647 • 95.803 • 1.044 * ( 29.'3 * .721 / IS.6)
VMSTD • ——i—........................................... m 56.552 03CF
( 66. » 460.)
VOLUME OP WATER VAPOR AT STANDARD CONDITIONS
VNC « .04707 * VLC
VWt « .OiTOT • 182. 6 " 875S SCF
PERCENT MOISTURE IN STACK CAS
BNO I'liOO.* V1CT / IVHSTO » VUC)
100. • S.56
> BMO » ——.................... • 12.T5 PERCENT
I 50.552 * 8.56
to
..^j ._... „ _ . _. , ..
03
MOLE TRACTION OF DRY STACK CAS
FMO • tlOO. • BNO) / 100.
.•«—..-..... • .872
100.
TkVERACE MOLfCUiAR iCICHT OF DRY STACK 6X8
MD * (PC02 • .44) » (P02 « .32) » (PN2 * PCO) • .28
MD * ( 4.00*44/100) * (11.0*32/100) * U85.0+ .0) * 28/100 • 29.08
MOLECULAR NEI6HT OP STACK CAS
MMS * MD * (1. - (BNO/100)) » 18. * (BNO/100)
MMS • 24.08* (I. -(12.75/100)) * 18. * (12.75/100) • 27.67
-------
STACK 6A8 VELOCITT AT STACK CONDITIONS
OELP • SUM. -OF THE SORT(VH • (TS • 460.))
VS • 85.49 • CP • OELP / (SORT(MKS * PS) • PNTS)
V3 • 6S. 49 • .64 * 91.155 / (SORT( 27.67 • 29.84) • 12. « 18.90 FPS
STACK 6AS VOLUMETRIC PLON AT STACK CONDITIONS
03 * VS • AS * 3600/144
OS • 18.98 * 7466. 3600/144 • 354354S. ACPH
STACK 6AS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSST6 * 17.647 * OS • P8~i 11. • (BMD/10V)) X CTS * 460.)
17.647 • 3543545. • 29.84 * (1. - (12.75/100))
OSSTD • — .... ..................................... ......... 1633313. SCFH
( 537. * 460.)
PERCENT ISOKINETIC
> ISO • (305.58*(TS«460.))M(0.002669«VLC)*(VM*V*(PB«fPM/13.6))/(TM*460.)))/(TT«V8*P8*DN*DN)
I
~ '(305. S8«(S37«-»460.))*( (0.002669* 182. )•( 55. 803*1. 0«4«( 29w93*( .721/13. 6))/( 66. •469.)))
ISO • ........ •—.—...————.—••——.———— .—..————.——— —....i-.———i. • 119.90 PERCENT
120. • 18.98 • 29.84 * .377 • ,377
PARTfCULAfE LOADINO « «PA METHOD 5 (AT 1TANOARD CONDITIONS)
CS « 0.001 • MN * 15.43 / VMSTD
CS » 0.001 • .0 • 15.43 / 58.552 » .000 0R/D8CF
PARTICULATE LB8/HR — EPA METHOD 5
PMR • CS * OSSTD / (15.43 • 453.6)
PMR • .000 * 1633313. / (15.43 * 453.6) • .00
-------
Run No. 7.?
Sample volume =1.66 m .58.55 scf
Example calculations
CS (Part) =187.1/1.66 = 112.7 mo/m3
CS (Part) = 0.001 xjj^jx 15.437 58.55.
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/
0.099 gr/dscf
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2$04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2$04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
187.1
3 Concentration,
mg/m
112.7
gr/dscf
0.049
1
ppm
A-240
-------
FIELD DATA
PLANT
SAMPLING LOCATION
REPUBLIC STEEL CLEVELAND
COKE OVEN OUTLET
SAMPLE TYPE 7-3-M8-S90
OPERATOR CLARKE
AMBIENT TEMP.(DEG.F) 52.
BAR.PRESS.(IN.HG) 27.92
STATIC PRESS.(IN.H20) -1.20
FILTER NUMBER(S) 3S30079
STACK INSIDE DIM.(IN) 97,50
PITOT TUBE COEFF. .94
THERM. NO.
LEAKA6E .000 CFM 9
METER CALIB. FACTOR .992
READ i RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME ~
(24-HR
CLOCK)
GAS METER
~ READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
00
3.0 IN.HG
ORIFICE PRESSURE STACK
DIFFERENTIAL TEMP
(IN.H20) (DE6.F)
DATE
RUN NUMBER
PROBE LENGTH • TYPE
NOZZLE I I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
'METER BOX NUMBER
METER HEAD OIFF.
C FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS. OIFF.
10/30/81
7-3
SFT GLASS HEATED
.394
12.0
FBI
1.27
.SB
350.
S50.
1.50
DRV GAS METER PUMP
TEMP VACUUM
(DEG.F) (IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPIN6ER
TEMP
(DEG.F)
DESIRED ACTUAL
INLET OUTLET
INIT
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110. 0
120.0
930
940
950
1000
1010
1020
1030
1040
1050
1100
1110
1120
~1130
TOTALS
AVERAGE
120.0
726.791
731.350
736.370
741.183
746.020
750.170
757.675
760.025
764.303
768.910
774.160
778.537
702.703
55.912
.060
.060
.060
.070
.050
.050
.070
.050
.050
.080
.050
.050
.72
.72
.72
.87
.62
.62
.67
.62
.62
.99
.62
.62
.72
.72
.72
.72
.87
.62
.62
.87
.62
.62
.99
.62
.62
916.
536.
550.
503.
507.
540.
536.
969.
562.
505.
916.
928.
.72 930.
56.
98.
63.
66.
69.
70.
72.
73.
74.
74.
74.
77.
69.
-92.
92.
52.
52.
•56.
.56.
.58.
-99.
60.
62.
.63.
•64.
=97.
.0
.0
.0
.0
.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
339.
386.
326.
346.
403.
396.
376.
382.
319.
331.
339.
357.
2.0 398.
44.
44.
46.
46.
50.
:54.
54.
52.
92.
90.
90.
'92.
90.
-------
PARTICIPATE FIELD DATA • RESULTS TABULATION
PLANT- NAME AND ADDRESS , TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
7-3
COKE OVEN OUTLET
to
TEST
TB
TF
TT
W-.
Y
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
ENGLISH UNITS
10/30/81
*30
1130
120.0
12
.992
•394 IN
••«
.72 IN-H20
METRIC UNITS
10/30/81
930
1130
120.0
12
.992
10.0 MM
.84
18.2 IMM-H20
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
VLC ~ T3TAL H»0 COLLECTED IN
IMPIN6ER8 AND SILICA 6El,ML.
VMC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRV
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL.* DRV
MD MOLECULAR NT-DAV STACK CAS
MMS MOLECULAR NT-STACK GAS
55.912 CU-FT
1.583 CU-M
63.0 F
52,351 SCF
ITfit
8.091 SCF
11.139
.866
4.00
11.00
.00
85.00
29.08
27.60
17.2
l.«»2
171.9
.229
13.39
.866
4.00
11.00
.00
85.00
29.08
27.60
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OP STACK 6*3
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK CAS VELOCITY
AS STACK AREA
OSSTD STACK PLON RATE, DRY*
OS ttTUAL STACK fLO* RAT8
ISO PERCENT I80KINETIC
MN PILTERABLE PART
M6. EPA 5
CS PILTERABLE PART
PMR PILTERABLE PART
EMISSION RATE
~i"~irBM'Ff'
IN.W6.
I
to
*>
u>
27
M
17
530
t«
7466
1573041
366206*
101
.92 IN-M6
.20 IN-M20
«83 IN-M6
P
.6 PP8
. 88-1N
. SCPH
. ACPH
.9
.0
.0000 OR/OSCP*
.000 L8/HR
709.17
-30.48
706.93
277.
6.0
4.817
44544.
103699.
101.9
.0
.000
.00
MM-HG
MM-H20
MM-HG
C
MRS
80-M
SCMH
ACMH
M6/D3C*
K6/HR
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 7-3
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD • (17.64? • VM * Y * (PB •» PM / 13.6)) / (TM * 460.)
IT.MT • 55.912 * .991 • ( 27.92 * ,716 / 13.6)
VMSTO « ...—-.—.......................................... • 52.351 03CF
( 63. * «60.)
VOLUME OF NATER VAPOR AT STANDARD CONDITIONS
VMC « .04707 • VLC
VKC •".WOT * 1TZ. • 8.0» ICF
PERCENT MOISTURE IN STACK BAS
BMO iTIOO. * VWCJ / IVMSTD » VNC)
& 100. * 8.09
I BNO • ...——»—..———...... * tl.3*» PERCENT
M 3Z.351 * B.09
(t^
^ ._ _ . .
MOLE FRACTION OF DRV STACK 6AS
FMD • (100. * BNO) / 100.
100. « 1S.4
FMD • ....................... • .86*
100.
~~AVERA3£ MOLCeuLAir REI6HT OF DRY STACK CAB
MO • (PC02 • .44) • (P02 • .32) * (PN2 • PCO) * .2$
MD • ( 4.00*44/100) • (11.0*32/100) * ((tS.O* .0) • 28/100 • 29.08
MOLECULAR NEI6HT OF STACK GAS
MMS • MO • (1. • (8*0/100)) * 18. • (BNO/100)
MNS » 29.08* (1. -(13.39/100)) 4 18. * (13.39/100) • 27.60
-------
STACK CAS VELOCITY AT STACK CONDITIONS
DELP • SUM. Of THE SORT(VH * (TS » 460.)I
VS • 85.49 • CP • DELP / (SORT(MMS • PS) • PNTS)
VS • 09.49 • .64 * 90.860 / (SORT( 27.60 • 27.83) • 12. • 19.62 FPS
STACK «A8 VOLUMETRIC FLOW AT STACK CONDITIONS
OS » VS * AS * 3600/144
OS • 19.62 • 7466. 3600/144 * 3662069. ACM
STACK 6AS VOLUMETRIC FLON AT STANDARD CONDITIONS
03STO • 17.647 * 08 • PS * (I. - (BMO/100)) / (TS * 460.)
17.647 • 3662069. * 27.83 • (I. - (13.39/100))
QS3TO • •-———i—•———-i—..—........—......... • 1373041. SCFH
( S30. * 460.)
I PERCENT ISOKINETIC
NJ
£ ISO « (305.58«(T8«460.))*((0.002669*VLC>«(VM*Y«(PB«(PM/13.6))/(TM«460.)))/(TT«VS*PS*DN*DN)
(305.S8*( 530.+460.))*((0.002669* 172.)+( 55.912* ,»92»( 27.92+( .718/13.6))/( 63.+460.)))
ISO • —.—.——.—..—....———.—.———.—..«—......................................... « 101.91 PERCENT
120. • 19.62 • 27.83 • .394 • .394
PAffTICUlATC LOADING — EPA METHOD 5 (*T 1TANOARD CONDITIONS)
CS • 0.001 • MN * 15.43 / VMSTO
CS « 0.001 * .0 * 15.43 / 52.351 • .000 6R/DSCF
PARTICULATE LBS/HR •• EPA METHOD 5
PMR • CS • OSSTD / (15.43 • 453.6)
PMR • .000 • 1373041. / (15.43 « 453.6) » .00
-------
Run No. 7.3
Sample volume =1.48 m3r 52.35scf
Example calculations
CS (Part) =64.8 71.48 = 43.fi mo/m3
CS (Part) « 0.001 X64.8 x 15.437 52.35= Q.niQ qr/dscf
3
CS (S02) = / = mg/m
= x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2SOA
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
64.8
- Concentration,
mg/m
43.8
gr/dscf
0.019
ppm
A-2 46.
-------
FIELD DAT*
I
NJ
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION COKE OVEN OUTLET
SAMPLE TYPE 7-4-MS-S50
OPERATOR CLARKE
AMBIENT TEMP. (DEB. F) 52.
BAR. PRESS. (IN. HG) 29.92
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 5530053
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .B4
THERM. NO.
LEAKAGE .015 CFM a 3.0 IN.HG
METER CALIB. FACTOR 1.016
READ » RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
INIT
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
ro.o
60.0
90.0
100.0
110.0
120.0
TIME
(24-HR
f*i nf*v i
CLUCK 1
933
943
953
1003
1013
1023
1033
1043
1053
1103
1113
1123
1133
READING
(CU.FT.)
142.828
147.074
151.900
156.405
161. SOI
165*595
170.186
175.043
177.365
1*3.575
18B.728
193.253
197.533
HEAD
(IN.H20)
. —
.060
.060
.060
.070
.050
.050
.070
.050
.050
.080
.050
-— .050
DIFFERENTIAL
(IN.
DESIRED
.T2
.72
.72
.87
.62
.62
.87
.62
.62
.99
.62
.62
H20)
ACTUAL
.72
.72
.72
.87
.62
.62
.87
.62
.62
.99
.62
.62
STACK
TEMP
(DEG.F)
928.
541.
557.
504.
528.
544.
547.
564.
564.
507.
518.
531.
DATE 10/30/81
RUN NUMBER 7-4
PROBE LENGTH t TYPE 6 FT GLASS HEATED
NOZZLE 1 1.0. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER
PETER BOX NUMBER FB5
METER HEAD DIFF. 1.86
C FACTOR .88
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
REFERENCE PRESS. DIFF. 1.50
DRV GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM
(DEC
INLET
60.
61.
65.
67.
71.
72.
76.
78.
78.
78.
80.
81.
.F) (IN.HG)
OUTLET
60.
60.
60.
61.
62.
65.
68.
70.
70.
71.
72.
73.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(DEG.F)
348.
390.
332.
346.
369.
350.
342.
340.
349.
350.
366.
354.
TEMP
(DEG.F)
36.
34.
32.
36.
40.
44.
43.
44.
46.
42.
•4.
46.
TOTALS
AVERAGE
120.0
54.705
.72
.72 536.
72.
66.
1.0 353.
41.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
7-4
COKE OVEN OUTLET
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1
*? VM
.00
TM
VMSTD
VLC
V"C
BMO
FMO
PC02
P02
PCO
PN2
MD
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL M«« COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRV
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR XT-STACK GAS
10/30/81
933
1133
120
12
1
54
69
55
161
7
12
4
11
85
29
27
.0
.016
.397 IN
.84
.72 IN-H20
.705 CU-FT
.1 F
.560 SCF
.1
.912 SCF
,«T
.875
.00
.00
.00
.00
.08
.70
METRIC UNITS
10/30/81
933
1133
120
12
1
10
1
20
1
168
12
4
11
85
29
27
.0
.016
.1
.84
.549
.6
.573
.1
.224
.47
.875
.00
.00
.00
.00
.08
.70
MM
iMM-H20
CU-M
C
3CM
SCM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OP STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOM RATE, DRT*
os ACTUAL STACK FLOM RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 66 DEC F, 29.92 IN.HG.
29.92 IN-H6
-1.20 IN-H20
29.03 IN-MO
536. F
I9.o rps
7466. 80-IN
1638107. SCFH
3340*82. ACFH
102.3
.0
.0000 GR/DSCF*
.000 LB/HR
T59.97 MM-HG
-30.48 MM-H20
757.73 »M-H6
280. C
5. 8 VP9
4.817 80-M
46386. SCHH
100267. ACMH
102.3
.0
.000
.00 KG/HR
M
^
VO
-------
Cn
o
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 7-4
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO i (17.647 * VM * Y • (PB * PM / IS.6)) / (TM * 460.)
17.647 * S4.703 * 1.016 • ( 29.92 * .716 / 13.6)
VMSTD » ————.———.———————.———— « 55.560 03CF
( 69. * 460.)
VOLUME OF WATER VAPOR AT STANDARD CONDITIONS
VNC • .04707 • VLC
VWC « .04707 * 166. » 7.91 SCF
PERCENT MOISTURE IN STACK GAS
BWO « (100. * VHCJ / (VMSTO » VHC)
100. * 7.91
BWO * ———.—————— t 12.47 PERCENT
55.560 * 7.91
MOLE FRACTION OF CRT STACK GAS
FMO « (100. • BNO) / 100.
100. • i*.5
FMO « ——•-•••••-—••••••« * .875
100.
AVERAGE MOLECULAR WEIGHT OF DRV STACK GAS
MO a (PC02 * .44) * (P02 « .32) » (PN2 «• PCO) • .26
MO s ( 4.00*44/100) * (1I.OOZ/100) • ((85.0* .0) • 28/100 * 29.08
MOLECULAR HEIGHT OF STACK GAS
MHS a MD * (1. - (BNO/100)) * 18. * (BNO/100)
MWS s 29.08* (1. -(12.47/100)) * 18. * (12.47/100) • 27.70
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP > SUM. OF THE 8QRT(VH • (T3 » 460.))
VS * 65.49 • CP • OELP / (SQRT(MN3 • PS) * PNTS)
VS 9 65.49 * .64 • 91.123 / (SORT( 27.70 * 29.63) * 12. • 16.97 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS « VS • AS • 3600/144
OS « 18.97 • 7466. 3600X144 • 3540602. ACPN
STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTD « 17.647 • OS • PS • (1. - (BNO/IOO)) / CT8 * 460.)
17.647 • 3540662. * 29.65 • (1. - (12.47/100))
OSSTO • ————.——————.————.—.—— * 1636107. SCFH
( 536. * 460.)
PERCENT ISOKINETIC
•f ISO • (305.58*(TS+460.))*((0.002669*VLC)*(VM*r*(PB+(PM/13.6))/(TM«460.)))/(TT*VS*P8*ON*DN)
tn (30S.56*( 536.«460.))M (0.0026*9* 160.)*( 54.705*1.016*( 29.92«( .710/13.6))/( 69.4460.)))
*-• ISO • -—————..—[[[ . |02.29 PERCENT
120. • 16.97 • 29.83 • .397 • .397
PARTICULATE LOADING — EPA METHOD 5 CAT STANDARD CONDITIONS)
CS * 0.001 * MN » 15.43 / VMSTO
CS » 0.001 * .0 • 15.43 / 55.560 » .000 6R/DSCF
PARTICULATE L0S/HR — EPA METHOD 5
-------
Run No. 7-4
*\
Sample volume =1-57 ^.55.56 scf
Example calculations
CS (Part) =62.6 / 1.57S 39.9 mq/m3
CS (Part) = 0.001 x 62-6 x 15.43755.56= 0.017 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2$04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2$04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
62.6
, Concentration,
mg/m
39.9
gr/dscf
0.017
ppm
A-252
-------
FIELD DATA
to
Ui
U)
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE STACK
SAMPLE TYPE METHOD 9-400
OPERATOR 00/MP
AMBIENT TEMP. (DEG.F) 50.
BAR. PRESS. (IN. HG) 29.92
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530035
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .64
THERM. NO.
LEAKAGE .018 CFM 8 12.
METER CALIB. FACTOR 1.033
READ ft RECORD DATA
TRAVERSE
POINT
NO.
IN It"
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
935
945
955
1005
1015
1025
1035
1045
1055
1105
1115
1125
1135
EVERY 10.0
GAS METER
READING
(CU.FT.)
•66.353
971.030
975.660
960.370
985.090
989.790
994.490
999.250
3.950
6.670
13.430
18.170
22.690
MINUTES
VELOCITY
HEAD
(IN.H20)
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
H20)
ACTUAL
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
STACK
TEMP
(DEG.F)
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
DATE 10/30/81
RUN NUMBER 7-5
PROBE LENGTH ft TYPE 6* GLASS
NOZZLE t 1.0. .374
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBER FB4
METER HEAD OIFF. t.aa
C FACTOR .92
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .18
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
S3.
-------
PARTICIPATE FIELD DATA • RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO/MP
TEST
7-5
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
1 VM
NJ
(J\ ...
TM
VMSTD
VLC
VNC
BNO
FMD
PC02
P02
PCO
PN2
MO
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF ORT CAS SAMPLED
AT STANDARD CONDITIONS*
~" TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
" PERCENT MOISTURE SY VOLUME
MOLE FRACTION ORT GAS
PERCENT C02 BT VOL., DRY
PERCENT 02 BY VOL., DRV
PERCENT CO BT VOL., ORT
PERCENT N2 BY VOL., DRV
MOLECULAR NT-DRV STACK GAS
MOLECULAR MT-STACK GAS
ENGLISH UNITS
10/30/81
"Ml
1135
120.0
12
1.033
.374 IN
.84
.72 IN-H20
56.537 CU-FT
66.9 F
56.631 SCF
"IB9.1
6.901 SCF
13.16
.868
4.00
11.00
.00
65.00
29.08
27.62
METRIC UNITS
10/30/81
935
1135
120.0
12
1.033
9.5
.84
16.3
1.601
19.4
1.660
189.1
.252
13.18
.868
4.00
11.00
.00
85.00
29.08
27.62
•MM
• H.N.
CU-M
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK CAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK GAS VELOCITY
AS STACK AREA
OSSTD STACK FLOW RATE, CRT*
OS ACTUAL STACK FLON RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA S
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68~ DEC F, 2*.92 tN.MC.
29.92 IN-H6
•1.20 1N-M20
29.83 IN-HG
S20. F
20.7 FPS
7466. 80*IN
1803803. SCFH
3867852. ACFH
110.5
.0
.0000 GR/DSCF*
.000 LB/HR
759.97 -KM-HG
•30.48 KM-H20
757.73 MM-MG
271. C
4.3 fPS
4.817 30-M
51078. SCHH
109520. ACMH
110.5
.0
.000 .CG/03CH
.00 KG/MR
NJ
cn
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 7*5
COKE STACK
VOLUME Of OUT 6AS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 * VM • Y • (PS * PM / 13.6)) / (TM » 460.)
17.6*7 • 56.537 * 1.033 » ( 29.92 * .710 / 13.6)
VMSTO • ————————.............................. . 58.631 D8CF
( 67. • 4*0.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 • VLC
VKC • .04707 • 189. • 8.90 SCF
PERCENT MOISTURE IN STACK 6AS
BHO * (100. * VMC) / (VMSTO * VHC) ~
100. * 8.90
BHO • —....................... * 13.18 PERCENT
jP S8.631 * 8.90
I
K>
cn
** MOLE FRACTION OF DRV STACK CAS
FMO » (100. • BMO) / 100.
IVO.-i~lI.ft ~
FMO « ——————.——. * .868
100.
AVERAGE MOLECULAR MEIOHT OF DRV STACK
MO » (PC02 * .44) * (P02 * .32) » (PN2 » PCO) • .26
MO « ( 4.00*44/100) * (11.0*32/100) * ((65.0* .0) • 26/100 « 29.08
MOLECULAR NEIGMT OF STACK CAS
MH3 • MD • (1. • (BNO/100)) * 16. * (BNO/100)
MMS « 29.06* (1. -(13.16/100)) * 18. • (13.16/100) « 27.62
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUN. OF THE SORTCVH * (TS » 466*))
VS » 85.49 • CP • OELP / (SORT(MWS • P8) * PUTS)
VS * 85.49 • .84 • 99.390 / (90RT( 17.62 * 29.83) • 12. • 20.72 FP3
STACK CAS VOLUMETRIC PLOW AT STACK CONDITIONS
03 • VS • AS • 3600/144
QS • 20.72 • 7466. 3600/144 » 3867652. ACFM
STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD » 17.647 • OS * PS * (1. • (BNO/iOO)) / (TS * 460.1
17.647 • 3867652. • 29.63 • (1. • (11.18/100))
OSSTD » ——————.................................... • 1803803. 3CFH
( 520. * 460.)
I PERCENT ISOKINETIC
to
^ ISO • (305.58MTS»460.))M(0.002669*VLC)*(VM«y*(PBt(PM/13.6))/(TM«460.)))/(TT*VS*P8*ON«ON)
(305.58M 520.»460.))«((0.002669* 189.)*( 56,537*1.033*( 29.92«( .720/13.6))/( 67.*460.)))
ISO « .————[[[i. . U0.46 PERCENT
120. • 20.72 • 29.83 • .374 • .374
PARTICULAR LOAOINC — EPA METHOD 5 CAT STANDARD CONDITIONS)
CS * 0.001 • MN * 15.43 / VMSTO
CS * 0.001 • .0 • 15.43 / 58.631 • .000 CR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
-------
Run No. 7.5
o
Sample volume =1.66 m T 58.63 scf
Example calculations
CS (Part) = 40.2/ 1.66= 24.2 mq/m3
CS (Part) = 0.001 x 40.2 x 15.43/58.63 = 0.010 qr/dscf
3
CS (S02) = / = mg/m
=_ x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
40.2
3 Concentration,
mg/m
24.2
gr/dscf
0.010
ppm
A-258
-------
FIELD DATA
to
PLANT REPUBLIC STEEL CLEVELAND
9AMPLIN6 LOCATION COKE STACK
SAMPLE TYPE METHOD 6*600
OPERATOR DO/MP
AMBIENT TEMP. (DEC. FJ so.
BAR. PRESS. (IN. HG) 29.92
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530215
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .64
THERM. NO.
LEAKAGE .000 CFM 8 6.0 IN.H6
METER CALIB. FACTOR .982
READ t RECORD DAT* EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK CAS METER VELOCITY ORIFICE PRESSURE
POINT TIME TIME READING HEAD DIFFERENTIAL
NO. (MIN.) (24-HR (CU.FT.) (IN.H20) (IN.H20)
INIT 0
10.0
20.0
30.0
40.0
50.0
60. 0
70.0
ao.o
90.0
100.0
110.0
120.0
l»fc.VVn/
934
944
954
1004
1014
1024
1034
1044
1054
1104
1114
1124
1134
421.124
425.840
430.460
435.190
439.950
444.670
449.400
454.130
458.620
463.510
468.200
472.970
477.636
DESIRED
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.42
.42
.42
.42
.42
.42
.42
.42
.42
.42
.42
.42
ACTUAL
.75
.75
.75
.75
.75
.75
.75
.75
.75
.75
.75
.75
STACK
TEMP
(DEG.F)
DATE 10/30/61
RUN NUMBER 7-6
PROBE LENGTH ft TYPE 4* QUARTZ
NOZZLE I I.D. .590
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBER FB8
METER HEAD OIFF. 1.91
C FACTOR .94
PROBE HEATER SETTING 250.
HEATER SOX SETTING 250.
REFERENCE PRESS. OIFF. .03
DRY GAS METER PUMP SAMPLE IMPINGES
TEMP VACUUM BOX TEMP TEMP
(DEG.F) (IN.HG) (OEG.F) (DEG.F)
INLET OUTLET
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
520.
47.
52.
57.
62.
65.
68.
69.
70.
70.
72.
73.
74.
46.
47.
49.
51.
•S3.
56.
58.
60.
61.
63.
63.
65.
3.1
3.2
3.7
4.0
4.2
4.2
4.3
5.2
6.3
7.3
7.7
7.9
615.
601.
593.
586.
565.
577.
574.
569.
571.
567.
590.
594.
38.
40.
40.
46.
52.
44.
44.
40.
40.
44.
44.
46.
TOTALS
AVERAGE
120.0
56.714
4.42
.75 520.
65.
56.
5.1 587.
43.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO/HP
TEST
7-*
COKE STACK
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
>
£ VM
o
TM
VMSTD
VLC
VNC
BMO
FMD
PC02
P02
PCO
PN2
MD
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL M20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRV
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRV
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
10/30/81
43*
1134
120
12
56
60
56
110
B
13
4
11
85
29
27
.0
.982
.590 IN
.84
.75 IN-H20
.714 CU-FT
.5 F
.604 SCF
,3
.487 SCF
.04
.870
.00
.00
.00
.00
.08
.64
METRIC UNITS
10/30/81
934
1134
120.
12
•
15.
•
19.
1.
IS.
1.
180.
•
13.
•
4.
11.
•
85.
29.
27.
0
982
0
84
1
606
8
603
3
240
04
870
00
00
00
00
08
64
.MM
MM-M20
CU-M
C
3CM
3CM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES Of STACK 0*3
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AV6 STACK 6*3 VELOCITY
AS STACK AREA
OSSTD STACK FLON RATE* DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
M6. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• fcT DEO f, 29.92 IK.MC.
29.92 IN-H6
•1.20 1N-M20
89.83 IN-H6
920. F
20.7 FPS
?«66. SO-IN
1806240. SCFM
ACFH
42.8
.0
.0000 8R/D3CF*
.000 LB/HR
739.97 MM-HG
•30.08 'MM-M20
T5T.73 'MM-H6
271. C
6.3 I«PS
4.817 SO-M
S1147. SCMH
109489. ACMH
42.8
.0
.000
.00 KG/MR
ro.
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 7-6
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 • VM • Y • (PB * PM / IS.6)) / (TM * 460.)
17.647 • 56.714 • .982 • ( 29.92 * .750 / 13.6)
VM3TD » •—....—.——..................................... • 56.604 DSCF
( 60. * 460.)
VOLUME OF NATER VAPOR AT STANDARD CONDITIONS
VNC * .04707 • VLC
VMC « .04707 • 180. • 8.49 SCP
PERCENT MOISTURE IN STACK GAS
BWO » UOO. * VWCJ / (VMSTO » VWC)
100. • 8.49
BMO a ....................——.. • 13.04 PERCENT
56.604 * 8.49
to
N MOLE FRACTION OF DRY STACK GAS
FMD » (100. - 8HO) / 100.
100. - 13.6
FMD a ....................... • .870
100.
~ AVERAGE MOLECULAR WEIGHT OF DRY STACK BAB
MO * (PC02 * .44) » (P02 • .32) * (PN2 * PCO) • .28
MO * ( 4.00*44/100) * (11.0*32/100) » ((85.0* .0) * 28/100 « 29.08
MOLECULAR WEIGHT OF STACK GAS
MWS * MD • (1. - (BNO/100)) « IB. • (BNO/100)
MWS a 29.06* (1. -(13.04/1001) •» 18. • (13.04/100) a 27.64
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP e SUM. OF THE SORT(VH • (TS •* 1*0.))
V3 « 85.49 • CP • DELP I (SORT(NWS • PS) • PNTS)
VS a 85.49 • .84 • 99.390 / (80RT( 27*64 • 29.83) * 12. » 20.71 FPS
STACK CAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS a VS • AS • 3600/144
OS « 26.71 * 7466. 3600/144 * 38665M. ACFH
STACK 6AS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD a 17.647 * OS • PS • (1. • (BNO/100)) / (TS « 460.)
17.647 • 3866549. • 29.83 • (1. - (13.04/100))
OSSTD a -------——————.——.—.———.—-— • 1806240. SCFH
( 520. * 460.)
PERCENT ISOKINETIC
ISO « (305.58«(TS»«60.))«((0.002669«VLC)*(VM*T»(PB*(PM/13.6))/(TM»«60.))}/(TT«V3«PS«DN«ON)
(305.38M S20.«460.))*((0.002669* 180.)*( S6.714* .982*( 29.92«( ,750/13.6))/( 60.«460.)))
ISO « ....—.—..—————.——.—..——..........—..—...................................—.. « 42.79 PERCENT
120. • 20.71 • 29.83 • .590 • ,590
PARTlCULATE LOA01NO " EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 • MN • 15.43 / VMSTD
CS a 0.001 * .0 • 15.43 / 56.604 a .000 6R/DSCF
PARTlCULATE LBS/HR — EPA METHOD 5
PMR a CS * OSSTD / (15.43 • 453.6)
PMR a .000 * 1806240. / (15.43 • 493.6) a .00
-------
Run No. 7.6
Sample volume = 1.60 m t 56.60 scf
Example calculations
CS (Part) =24.3/1.60=15.2 mq/m3
CS (Part) = 0.001 x24-3 x 15.43/ 56.60= 0.007 qr/dscf
.3
CS (S02) = / = mg/nT
= x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
24.3
3 Concentration,
mg/m
15.2
gr/dscf
0.007
ppm
A-264
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEC.F)
BAR.PRESS.(IN.H6)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
COKE OVEN OUTLET
6-3-M8-350
CLARKE
65.
29.93
-1.20
3530061
97.90 .00
.84
.000 CFM
.992
3.0 IN.HG
READ & RECORD DATA EVERT 10.0 MINUTES
DATE
RUN NUMBER
PROBE LENGTH I TYPE
NOZZLE I I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER
METER MEAD DIFF.
c FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS. DIFF.
to/so/ai
8-1
« FT GLASS HEATED
.378
12. 0
FBI
1.87
.88
350.
350.
1.50
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
CLUCK J
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H20)
DESIRED ACTUAL
STACK
TEMP
(OEG.F)
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(OEG.F)
IMPINGER
TEMP
(DEG.F)
INIT
CTi
U1
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
1438
1448
1458
1508
1518
1528
1538
1548
1608
1618
1628
1638,
1648a
TOTALS
AVERAGE
120.0
783.033
787.530
792*020
796.760
801.150
805.468
810.000
814.800
819.987
824.901
829.699
834.999
840.297
57.264
.090
.050
.060
.050
.050
.050
.060
.070
.060
.060
.070
.070
.62
.62
.73
.62
.62
.62
.73
.87
.T3
.73
.87
.62
.62
.73
.62
.62
.62
.73
.87
.73
.73
.87
.87
540.
558.
570.
519.
530.
537.
542.
559.
575.
526.
536.
546.
.72 545.
75,
76.
80,
82.
83.
64.
86.
86.
86.
86.
86.
86.
83.
70.
69.
70.
71.
72.
72.
73.
74.
74.
74.
74.
74.
78.
2.0
2.0
2.0
3.0
2.0
2.0
2.0
2.0
2.0
3.0
3.0
3.0
319.
347.
320.
332.
289.
298.
314.
342.
351.
351.
365.
359.
2.3 332.
56.
56.
56.
58.
60.
58.
58.
58.
98.
58.
57.
58.
58.
Vinal time should be 1638.
-------
PARTICIPATE FIELD DATA • RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
e-i
COKE OVEN OUTLET
TEST
TB
TF
TT
NP
V
ON
CP
PM
1
to VM
O^
O^ •
TM
VMSTD
VLC
VNC
BNO
FMD
PC02
P02
PCO
PN2
MO
MMS
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MtN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL M20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRV
PERCENT 02 BY VOL.* DRY
PERCENT CO BY VOL., DRV
PERCENT N2 BY VOL., DRV
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
10/30/81
1438
1648
110,0
12
.992
.378 IN
.84
.72 IN-M20
97.264 CU-FT
77.6 F
55.906 SCF
W.8
9.405 SCF
14.40
.656
4.30
9,30
.00
86.40
29.06
27.47
METRIC UNITS
10/30/81
1438
1648
120.0
12
.992
9.6 'MM
.84
18.3 MM-H20
1.622 CU-M
25.3 C
1.583 SCM
199.8
.266 SCM
14.40
.836
4.30
9.30
.00
86.40
29.06
27.47
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK CAS
PS STACK PRES, ABS.
T3 AVERA6E STACK TEMP
VS AV6 STACK 6AS VELOCITY
AS STACK AREA
QSSTD STACK FLOW RATE* DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 66 DEO F, 29.92 1N.H6.
29.93 IN-H6
-1.20 IN-MZO
89.64 IN-H6
S«5. F
19.Z FPS
7466. SQ-IN
U04S20. 8CFH
ACFN
IIS.9
.0
.0009 6R/OSCF*
.000 LB/HR
2 MM-H6
•30.48 HM-M20
737.98 MM«H6
285. C
5.8 MPS
4.817 SO-M
45435. SCMH
101278. ACMH
115.9
.0
.000 ne/oso
.00 K6/HR
>
to
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 8-1
COKE OVEN OUTLET
VOLUME OF DRV CAS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.647 • VM • T • (Pfl * PM / IS. 6)) / (TM * 460.)
17.647 • 57.264 • .992 * ( 29.93 * .719 / 13.6)
VMSTD « —————.— ———...— ........... ............. • 55.906 OSCF
( 78. * 460.)
VOLUME Of HATER VAPOR AT STANDARD CONDITIONS
VMC • .04707 • VLC
VNC « .0*707 • 200. m 9.40
PERCENT MOISTURE IN STACK CAS
BHO * (100. * VNC) / (VMSTD * VHC)
te 100. * 9.40
7 BHO « ———.—....— ........ • 14.40 PERCENT
NJ 55.906 • 9.40
oo
MOLE FRACTION OP DRV STACK 6AS
FMD « (100. . BNO) / 100.
- 100. - I*.i
FMD » —.«-.-.••——-—•• • .896
100.
*VER*6E MOLECULAR NEIGHT OF DRV STACK 6AS
MO * (PCOZ * .44) • (P02 * .32) » (PN2 » PCO) * .20
MD * ( 4.30*44/100) * ( 9.3*32/100) * ((86.4* .0) * 28/100 * 29.06
MOLECULAR NEI6HT OF STACK CAS
MHS » MD • (1. • (BMO/100)) * 18. • (BNO/100)
MMS i 29.06* (1. -(14.40/100)) * 18. * (14.40/100) • 27.47
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. Of THE 8QRT(VH • (TS * 460.))
VS « 85.49 • CP • OELP / (SORT(MNS * F8) • PNTS)
V3 » 85.49 * .84 • 91.672 / (SQRT( (7.4? • 29.84) • 12. • 19.16 FPS
STACK 6AS VOLUMETRIC PLOW AT STACK CONDITIONS
03 > VS • AS • 3600/144
OS * 19.16 • TI66. 3600/144 • 357(567. ACPM
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD • 17.647 • OS • PS * Cl. - (BNO/100)) / (T8 » «60.)
17.647 * 3576587. • 29.04 • (1. • (14.40/100))
OSSTD • .—.—...————....—...........———— • 1604520. 3CFH
( 545. » 460.)
PERCENT ISOKINETIC
"T ISO » (305.3«<>(TS«460.))*((0.00*669*VLC)*(VM*Y*(PB*(PM/13.6))/(TM«460.)))/(TT«VS*M*DN*DN)
to
2 " (30*.«Mr*««.»*60.))«((0.002i4>«i 200. )*( 57.264* .992«( 29.93*( .719/13.6))/( 7B.*fl60.)))
ISO » —.—...——.—.——..—......—.......—................................................. • 115.92 PERCENT
120. • 19.16 * 29.84 • .378 * .378
PARTiCULAtt LOADING — EPA METHOD 5 IAT STANDARD CONDITIONS)
CS « 0.001 • MN * 15.43 / VMSTD
CS » 0.001 * .0 * 15.43 / 55.906 * .000 GR/DSCF
PARTICIPATE LBS/HR •" EPA METHOD 5
PMR * CS * OSSTD / (15.43 • 453.*)
PMR r .000 • 1604520. / (15.43 * 453.6) * .00
-------
Run No. 8.1
3
Sample volume = 1.58 m T 55.91 scf
Example calculations
CS (Part) = 65.3/1.58 = 41.^ mq/m
CS (Part) = 0.001 X65.3 x 15.43/ 55.91=
3
n.Dia qr/dscf
CS (S02)
= x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sul f uric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
65.3
3 Concentration,
mg/m
41.3
gr/dscf
0.018
ppm
A-270
-------
FIELD DATA
PLANT
SAMPLING LOCATION
REPUBLIC STEEL CLEVELAND
COKE OVEN OUTLET
DATE
NUMBER
10/30/81
e-2
SAMPLE TYPE 8-2-M5-350
OPERATOR CLARKE
AMBIENT TEMP.(OEG.F) 65.
BAR. PRESS. (IN.HG) 29.93
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530034
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 3.
METER CALIB. FACTOR 1.016
READ & RECORD DATA EVERT 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT TIME
NO. (MIN.)
INIT 0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
TIME
(24-HR
1441
1451
1501
1511
1521
1331
1541
Ib51
1601
1611
1621
1631
1641
READING
(CU.FT.)
197.754
202.330
206.710
211.485
215.873
220.536
224.460
229. 31b
234.210
238.500
243.000
248.026
253.000
HEAD
(IN.H20)
—
.050
.050
.060
.050
.050
— .050
.060
.070
.060
.060
.070
.070
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.62
.62
.73
.62
.62
.62
.73
.87
.73
.73
.87
.87
H20)
ACTUAL
.62
.62
.73
.62
.62
.62
.73
.87
.73
.73
.87
.87
STACK
TEMP
(DEG.F)
540.
559.
570.
521.
529.
540.
546.
563.
518.
529.
540.
547.
PROBE LENGTH ft TYPE 5 FT GLASS HEA
NOZZLE : 1.0. .397
ASSUMED MOISTURt 12.0
SAMPLE BOX NUMBER
METER BOX NUMBER FB5
METER HEAD OIFF. 1.86
C FACTOR .88
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
REFERENCE PRESS. DIFF. 1.50
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM
(DEG
INLET
85.
85.
87.
A9.
90.
91.
90.
90.
91.
90.
90.
90.
.F) (IN.HG)
OUTLET
84.
84.
84.
84.
84.
80.
84.
83.
83.
83.
83.
83.
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
.0
BOX TEMP
(DEG.F)
338.
364.
343.
338.
315.
319.
305.
319.
329.
346.
361.
352.
TEMP
(DEG.F)
50.
48.
46.
46.
46.
44.
46.
44.
46.
40.
44.
45.
TOTALS
AVERAGE
120.0
55.246
.72
.72 542.
89.
84.
1.0
336.
46,
-------
ro
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND CLARKE
TEST
e-2
COKE OVEN OUTLET
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
VM
TM
VMSTD
VLC
VNC
BNO
FMD
PC02
POZ
PCO
PN2
MO
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BY VOL.r DRV
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRV
PERCENT N2 BV VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR XT-STACK GAS
10/30/81
1441
1641
120
12
1
55
06
54
206
9
15
. *
4
9
86
29
27
.0
.016
.397 IN
.84
.72 IN-H20
.246 CU-FT
.3 F
.364 SCF
.2
.706 SCF
.15
.849
.30
.30
.00
.40
.06
.38
METRIC UNITS
10/30/81
1441
1641
120.
12
1.
10.
"
18.
1.
30.
1.
206.
•
15.
.
4.
9.
.
86.
29.
27.
0
016
1
8Q
3
564
2
539
2
275
15
849
30
30
00
40
06
38
KM
PM-H20
CU-M
C
SCM
SCM
-------
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
08STD STACK PLOW RATE* DRY*
OS ACTUAL STACK FLOH RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MG. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
* 68 DEC F, 29.92 1N.H6.
29.93 IN-HG
-1.20 IN-H20
29.64 IN-HG
542. F
19.2 FPS
7466. SO-IN
15*5254. SCFH
3576610. ACFH
102.8
.0
.0000 GR/OSCF*
.000 LB/HR
760.22 KM-HG
-30.08 CM-M20
T57.98 KM-HR
283. C
5.8 VPS
4.817 SO-M
45175. SO'H
101279. AC^H
102.8
.0
.000 PG/DSCP
.00 KG/HR
to
~4
U)
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. e-a
COKE OVEN OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO * (17.647 * VH * T * (PB * PM / Hi6)) / (TM * 460.)
17.647 • 55.346 • 1.016 * ( 24.93 + .719 / 13.6)
VMSTD * — — — — - ------ — — . ---- ..... -------------------- - 54.364 DSCF
( 86. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC * .04707 • VLC
VRC *~.04707 * 206; a ^.7
PERCENT MOISTURE IN STACK GAS
~ BWO *"UOO. » VHCr / tVWSTO * VWC)
100. * 9.71
BHO «————"--—— ---- . ft 15.15 PERCENT
S4.364 + 9.71
>
1 .......... " -....-.... . . ..... ,_
to
4* MOLE FRACTION OF DRV STACK GAS
FMO = (100. - BHO) / 100.
100. * 15.1
FMD « .-.——..-— ......... - .849
100.
AVERAGE MOLECULAR WEIGHT OF ORT STACK GAS —
MO = (PC02 * .44) * (P02 * .32) * (PN2 » PCO) • .28
MO * ( 4.30*44/100) * ( 9.3*32/100) * ((86.4* .0) * 26/100 * 29.06
MOLECULAR HEIGHT OF STACK GAS
MHS a MD • (i. - (BMO/ioo)) * is. * (BNO/IOO)
MHS a 29.06* (1. *(15.15/100)) » 18. • "(15.15/100) • 27.38
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SORT(VH * (TS * 060.))
VS = 95.49 • CP • OELP / (SORT(MNS * PS) • PNTS)
VS s 85.49 • .80 • 91.534 / (30RT( 27.38 * 39.80) * 12. « 19.16 FPS
STACK 6AS VOLUMETRIC FLO* AT STACK CONDITIONS
OS s VS • AS * 3600/144
OS = 19.16 * 7466. 3600/144 * 357««10. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD * 17.647 • OS • PS • (!;-» (BNO/tOO)) / (TS * 460.)
17.647 » 3576610. * 29.84 • (I. - (15.15/100))
OSSTD * —— ——— ..................... .. . x 1595254. SCFH
( 542. «• 460.)
> PERCENT ISOKINETIC
^ ISO « (305.58*(TS»460.))«((0.002669»VLC)«(VM»r«(PB«(PM/13.6))/(TM«460.)))/(TT«VS<»P3«DN*DN)
cn
(305.58*( 542.*460.))M(0.002669" 206.)»( 55.246*1.016*( 29.93»( .719/13.6))/( 86.*460.)))
130 » .......................... .............. . ............................ . .... • 102.78 PERCENT
1?0. • 19.16 • 29.84 « .397 • .397
PARTICIPATE LOADING »* EPA METHOD 5 (AT STANDARD CONDITIONS)
CS c 0.001 • MN • 15.43 / VMSTO
CS = 0.001 • .0 • 15.43 / 54.364 « .000 GR/DSCF
PARTICULAR LBS/HR — EPA METHOD 5
PMR « CS * OSSTD / (15.43 * 453.6)
PMR • .000 * 1595254. / (15.43 • 453.6) * .00
-------
Run No. 8.2
Sample volume =1.54 m t 54.36 scf
Example calculations
CS (Part) =76.0/1.54 g 49.4 mq/m3
CS (Part) = 0.001 x 76.0 x 15.43/54.36 = 0.022 qr/dscf
3
CS (S02) = / = mg/m
= x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
76.0
3 Concentration,
mg/m
49.4
gr/dscf
0.022
ppm
A-276
-------
FIELD DATA
N>
~
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.t COKE BATTERY OUTLET
SAMPLE TYPE PART/H2304/302
OPERATOR BRUFFEY
AMBIENT TEMP, (DEC. F) 78.
BAR. PRESS. (IN. H6) 29.93
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530120
STACK INSIDE DIM. (IN) 47.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM a 9.0 IN.H6
METER CALIB. FACTOR 1.003
READ t RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK CAS METER VELOCITY ORIFICE PRESSURE
POINT
NO.
iNlf"
TIME
(MIN.)
0
10.0
20.0
30.0
00. 0
50.0
60.0
70,0
80.0
90.0
100.0
110.0
120.0
TIME
(24-HR
f*l flfftf %
CLUCK/
1418
1448
1458
1508
1518
1528
1538
1548
1558
1608
1618
1628
1638
READING
(CU.FT.)
48.689
S3. 490
58.200
63.360
68.090
72.820
77.640
82.800
88.390
93.580
98.750
104.320
109.886
HEAD
(IN.H20)
—
.050
.050
.060
.050
.050
.050
.060
.070
.060
.060
.070
.070
DIFFERENTIAL
(IN.
DESIRED
.62
.62
.T3
.«2
.62
.62
.73
,87
.73
.73
.87
.S7
H20)
ACTUAL
.62
.62
,T3
.62
.62
.62
.73
,•7
.73
,73
.87
,«7
STACK
TEMP
(DE6.F)
540.
558.
570.
519.
530.
537.
543.
559.
575.
527.
538.
545.
DATE 10/30/81
RUN NUMBER 8-3
PROBE LENGTH • TYPE 5* HEATED GLASS
NOZZLE I 1.0. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER 0
METER BOX NUMBER FB2
METER HEAD DIFF. 1.76
C FACTOR .86
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
REFERENCE PRESS. DIFF. .15
DRY GAS 'METER PUMP SAMPLE IMPINGER
TEMP
(DE6
INLET
76.
77.
81.
83.
85.
86.
87.
88.
89.
88.
87.
87.
.F)
OUTLET
74.
75.
76.
77.
78.
79.
80.
80.
81.
82.
82.
81.
VACUUM
(IN.HG)
2.0
2.0
2.0
2.5
2.5
3.0
3.0
3.0
4.5
4.5
4.5
4.0
BOX TEMP
(DE6.F)
354.
376.
388.
387.
367.
368,
387,
400.
406.
404.
408.
409,
TEMP
(DE6.F)
49.
52,
55.
56.
57.
59.
61.
60.
66.
69.
67.
65.
TOTALS
AVERAGE
120.0
61.197
.72
.72 545.
SS.
79.
3.1 388.
60,
-------
PARTICULATE FIELD DATA S RESULTS TABULATION
PLANT* NAME AND ADDRESS TCST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
8-3
NO.l COKE BATTERY OUTLET
TEST DATE
TB
TF
TT
NP
V
ON
CP
PM
¥ VM
to
" TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
ENGLISH UNITS
10/30/81
1436
1638
120.0
12
1.003
.397 IN
.84
.72 IN-H20
61.197 CU-FT
81.6 F
59.962 SCF
METRIC UNITS
10/30/61
1438
1638
120.0
12
1.003
10.1 MM
.64
18.3 ,MM-H20
1.733 CU-M
27.6 C
1.696 SCM
AT STANDARD CONDITIONS*
VLC "TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA 6EL»ML.
VNC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
6*6 PERCENT MOISTURE 6V VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRV
P02 PERCENT 02 BY VOL.* DRV
PCO PERCENT CO BV VOL., DRV
PN2 PERCENT N2 BV VOL., DRV
MO MOLECULAR MT-DRV STACK GAS
MNS MOLECULAR MT-STACK GAS
(89.4
6.915 SCF
169.4
.252 SCM
12.94
.871
4.30
9,30
.00
66.40
29.06
27.63
12.94
.871
4.30
9.30
.00
86.40
29.06
27,63
-------
PB
PSI
PS
TS
VS
AS
QSSTD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES Of STACK CAS
STACK PRESt ABS.
AVERAGE STACK TEMP
AVC STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE* DRY*
ACTUAL STACK F LOW RATE
PERCENT ISOKINETIC
FILTERABLE PART
MG. EPA 5
FILTERABLE PART
FILTERABLE PART
EMISSION RATE
29.93 IN-H6
•1.20 IN-MZO
29.60 IN-HG
8*5. F
FPS
30-IN
SCFH
ACFH
19.1
7466.
1626862.
3566*12.
111.2
.0
.0000 6R/08CF*
.000
760.22 MM-HG
-30.08 MM*H20
757.98 MM-HC
285. C
5.8 VPS
•.617 80-M
46068. SCMH
100996. ACMH
111.2
.0
.000 MG/OSCK
.00 KG/HR
* 68 DEC f,
1N.H6.
NJ
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 6-3
NO.l COKE BATTERY OUTLET
VOLUME OP DRY CAS SAMPLED AT STANDARD CONDITIONS
VM3TD • (17.647 * VM « V * (PB • PM / 13.6)) / (TM * 460.)
17.647 * 61.197 * 1.003 * ( 29.93 * .719 / 13.6)
VMSTD • —.-.——————.-•—— ......... .............. * 59.962 D3CF
( 62. » 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC • .04707 • VLC
VHC » .WTOT • 189. • 8.92 SCF
PERCENT MOISTURE IN STACK GAS
BHO » (100. * VNC) 1 (VMSTD * VMC)
100. • a. 92
..... • 12. 94 PERCENT
jp 59.962 * 8.92
fo
00
° MOLE FRACTION OF DRY STACK GAS
FMO » (100. > BNO) / 100.
100. - 12.9
FMO « — — ................. • .871
100.
AVERAGE MOLECULAR MEI6HT OF DRY STACK BIB
MD * (PC02 • .44) « (P02 • .32) * (PN2 * PCO) • .28
MO * ( 4.30*44/100) » ( 9.3*32/100) * ((86.4+ .0) * 28/100 * 29.06
MOLECULAR NEI6MT OF STACK GAS
MMS * MD • (1. • (8X0/100)) + 18. • (BNO/100)
MWS « 29.06* (1. -(12.94/100)) • 18. * (12.94/100) * 27.63
-------
STACK 6A3 VELOCITY AT STACK CONDITIONS
DELP » SUM. OF THE SQRT(VH * (TS » 460.))
VS * 65.49 • CP • OELP / (SORT(M*S • PS) • PNTS)
VS ' BS. 49 * .84 * 91.684 / (30RT( 27.63 * 29.84) • 12. « 19.11 FP3
STACK GAS VOLUMETRIC PLOD AT STACK CONDITIONS
QS a VS * AS • 3600/144
OS « 1*. ii • 7466. 3600/144 • 356*612. ACFH
STACK CAS VOLUMETRIC FLO* AT STANDARD CONDITIONS
OSSTD i 17.647 * 69 * PS • (1. - (BNO/100)) / (T8 * 460.)
17.647 * 3566612. • 29.84 • (1. • (12.94/100))
OSSTD « —————.———— ........... .......... --- ... « 1626862. SCFH
( 545. » 460.)
> PERCENT ISOKINETIC
ISO « (305.58*(TS«460.))*((0.002669*VLC)*(VM*Y*(P8«(PM/13.6))/(TM«460.)))/(TT*V8*PS*DN«DN)
(3D5.58«( 5«5.M60.))*((0. 002669* 189. )*l 61. 197*1. 003«( 29.93*( . 719/13. 6))/( 82.*460.)))
ISO •--.---..-------.--------.-.------.——————————————•————————— * 111. 16 PERCENT
120. * 19.11 * 29.84 • ,397 • .397
PARTlCULlTE LOADING — EPA METHOD 5 1*T"1T*NDAHO CONDITIONS)
C3 » 0.001 • MN * 15.43 / VMSTD
CS * 0.001 • .0 * 15.43 / 59.962 « .000 6R/DSCF
PARTICULATE LBS/HR « EPA METHOD 5
PMR « CS • OSSTD / (15.43 • 453.6)
PMR • .000 * 1626862. / (15.43 • 453.6) • .00
-------
Run No. 8.3
Sample volume = 1.70 m . 59.96 scf
Example calculations
CS (Part) = 66.17 1.70= 38.9 mq/m3
CS (Part) = 0.001 x 66.1 x 15.43/59.96 = 0.017 qr/dscf
.3
CS (S02) = / = mg/nT
- x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2$04
As H2$04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
66.1
3 Concentration,
mg/m
38.9
gr/dscf
0.017
ppm
A-282
-------
FIELD DATA
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PART
OPERATOR BRUFFKY
AMBIENT TEMP. (DEC. r) 76.
BAR. PRESS. (IN. H6) 29.93
STATIC PRE3S.UN.HZO) -1.20
FILTER NUMBER(S) 3530117
STACK INSIDE DIM. (IN) 97. SO .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .890 CFM 8 3.0 IN.H6
METER CALIB. FACTOR 1.044
READ « RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE
POINT ~ TIME
NO. (MIN.)
fji|T 0
a* 10-°
7 20.0
M 30.0
a* 40.0
w 50.0
60.0
70.0
SO.O
90.0
100.0
110.0
120.0
TIME"
(24-HR
n nnr i
vLUln J
1M1
1451
1501
1510
1520
1531
1541
1551
1601
1611
1621
1631
1641
READING
(CU.FT.)
260.098
265.580
269. 9ZO
274.780
279.070
283.450
287.830
292.580
297.760
302.530
307.200
312.460
317.529
HEAD
(IN.H20)
- ..
.050
.050
.060
.050
.050
.050
.060
.070
.060
.060
.070
.070
DIFFERENTIAL
(IN.
DESIRED
.62
.62
.73
.62
.62
.62
.73
.87
.73
.73
.87
.87
H20)
ACTUAL
.62
.62
.73
.62
.62
.62
.73
.87
.73
.73
.87
.87
STACK
TEPP
(DEG.F)
540.
558.
564.
525.
530.
540.
547.
564.
580.
529.
544.
547.
DATE 10/30/81
RUN NUMBER 8-4
PROBE LENGTH S TYPE 4' HEATED GLASS
NOZZLE 1 I.D. .397
ASSUMED MOISTURE 12.0
SAMPLE BOX NUMBER 0
METER BOX NUMBER FIO
METER HEAD OIFF. i.so
C FACTOR .86
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
REFERENCE PRESS. OIFF. .15
DRY GAS METER PUMP SAMPLE IMPIN6ER
TEMP
(DEG
INLET
90.
91.
94.
96.
97.
97.
97.
78.
97.
97.
97.
96.
.F)
OUTLET
90.
91.
92.
92.
93.
93.
93.
94.
93.
93.
93.
92.
VACUUM
(IN.HG)
1.0
1.5
2.0
2.0
2.0
3.0
4.0
4.5
4.0
4.5
5.0
5.0
BOX TEMP
(DEG.F)
392.
398.
406.
348.
359.
377.
403.
413.
404.
406.
405.
407.
TEMP
(DEG.F)
92.
S3.
55.
57.
56.
99.
60.
64.
66.
68.
66.
64.
TOTALS
AVERAGE
120.0
56.631
.72
.72 S47.
94.
92.
3.2 393.
60.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST
0-4
NO.l COKE BATTERT OUTLET
KJ
00
TEST
TB
TF
TT
NP
T
ON
CP
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST* MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
ENGLISH UNITS
10/30/81 '
1441
1641
120.0
12
1.044
.397 IN
.84
METRIC UNITS
10/30/81
1441
1641
120.0
12
1.044
10.1 MM
.84
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL M20 COLLECTED IN
IMPINGERS AND SILICA CEL.ML.
VNC VOLUME OF WATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRV
P02 PERCENT 02 BY VOL.* DRV
PCO PERCENT CO BY VOL.* DRV
PN2 PERCENT N2 BY VOL.* DRY
MO MOLECULAR WT-ORV STACK GAS
MMS MOLECULAR HT-STACK GAS
.72 IN-H20
56.631 CU-FT
18.3 IMM-H20
1.604 CU-M
93.2 F
56.551 SCF
^1.3
9.004 SCF
13.74
.863
4.30
9.30
.00
86.40
29.06
27.54
34.
1.
191.
•
13.
•
4.
9.
•
86.
29.
27.
0 C
601 SCM
3
255 SCM
74
863
30
30
00
40
06
54
-------
fO
CO
en
PB BAROMETRIC PRESSURE
PSI STATIC PRES OF STACK GAS
PS STACK PRES, ABS.
TS AVERAGE STACK TEMP
VS AVG STACK GAS VELOCITY
AS STACK AREA
OSSTO STACK FLOW RATE* DRY*
OS ACTUAL STACK FLOW RATE
ISO PERCENT ISOKINETIC
UN FILTERABLE PART
MS. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 48 DEC F, 29.92 IN.M8.
29.93 IN-H6
•1.20 IN-H20
29.B4 IN-M6
547. F
19.2 FPS
7466. SO-IN
1*12867. SCFH
3S76390. ACFH
109.8
.0
.0000 GR/DSCF*
.000 LB/MR
760.22 MM-HG
•30.48 HM-H20
757.98 MM-HG
266. C
5.8 MPS
4.817 30-M
45672. 3CHH
101273. ACMH
105.8
.0
.000 M6/DSCK
.00 KG/HR
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 8-0
NO.l COKE BATTERY OUTLET
VOLUME OP DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 * VM • Y • (P8 * PM / 13.6)) / (TM » 460.)
17.647 • 56.631 * U044 * ( 29.93 * .719 / 13.6)
VMSTO « .—————.-——.—.—.—.—-.—— ... • 86.551 OSCP
( 93. * 460.)
VOLUME OP WATER VAPOR AT STANDARD CONDITIONS
VNC « .04707 • VLC
VMC • .04707 • 191. • 9.00 SCF
PERCENT MOISTURE IN STACK GAS
BMO « (iOO, * VHC) / CVMSTD » VWC)
^ 100. • 9.00
7 BMO « —.......—..————.. • 13.74 PERCENT
M 56.551 * 9.00
GO
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE 8QRT(VH • (TS * 460.))
VS « 85.49 • CP • OELP / (SQRT(MKS • PS) * PNTS)
VS * 85.49 * .84 • 91.790 / (SORT( 27.54 * 29.84) • 12. • 19.16 FPS
STACK 6AS VOLUMETRIC FLO* AT STACK CONDITIONS
03 « VS • A$ • 3690/144
08 a 19.16 • 7466. 3600/144 » 3576390. ACFH
STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO * 17.647 • OS * P8 • (1. - (BMO/100)) / (T8 «• 460.)
17.647 • 3576390. * 29.84 • (1. - (13.74/100))
OSSTO • i.i—........................................ .. * 1612867. 3CFH
( 547. » 460.)
•p PERCENT ISOKINETIC
NJ ISO * (30S,5eMTS»460.))«((0.002669«VLC) + (VM*Y«(PB»(PM/13.6))/(TM*«60.)))/(TT«VSOPS<»DN«ON)
oo • •
^ (305.58«( 547.*460.))*((0.002t»f* 191.)*( 56.631*1.040*( 29.93«( .719/13.6))/( 93.*«60.)))
ISO « ....—[[[ « 105.75 PERCENT
120. * 19.16 • 29.84 • .347 * .397
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
C8 « 0.001 • MN • 15.43 / VMSTD
CS • 0.001 • .0 * 15.43 / 56.551 • .000 6R/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
-------
Run No. 8.4
Sample volume = 1.60 m3t 56.55 scf
Example calculations
CS (Part) = 60.5/ 1.60= 37.8 mo/m3
CS (Part) = 0.001 x60.5 x 15.43/56.55 = 0.016qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
60.5
3 Concentration,
mg/m
37.8
gr/dscf
0.016
i
ppm
A-288
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEC.F)
BAR.PRESS.(IN.H6)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
COKE STACK
METHOD 3-250
00/MP
67.
-1.20
3530008
97.50
.84
.00
.020 CFM 8 19.5 IN.HG
1.033
DATE 10/30/81
RUN NUMBER 8-5
PROBE LENGTH t TYPE 6* GLASS
NOZZLE I 1.0. .374
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
'METER BOX NUMBER PB4
METER HEAD OIFF. 1.88
C FACTOR .92
PROBE HEATER SETTING 290.
HEATER BOX SETTING 290.
REFERENCE PRESS. OIFF. .18
READ t RECORD DATA EVERT 10.0 MINUTES
1
>
NJ
00
vo - •-
TRAVERSE SAMPLE
POINT TIME
NO. (MIN.)
INIf 0
10.0
20.0
30.0
«0.0
90.0
60.0
70.0
80.0
90.0
100.0
104.2
CLOCK
TIME
(24-HR
CLOCK)
1439
1449
1459
1509
1519
1529
1539
1549
1999
1609
1619
1623
GAS METER
READING
(CU.FT.)
VELOCITY ORIFICE PRESSURE
HEAD DIFFERENTIAL
(IN.H20) (IN.H20)
DESIRED
23.414
28.190
32.880
37.600
42.320
47.040
91.740
56.440
61.150
65.860
70.590
72*492
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.070
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
ACTUAL
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
.72
STACK
TEMP
(DEG.F)
DRV GAS METER PUMP SAMPLE
TEMP VACUUM BOX TEMP
(DEG.F) (IN.HG) (DEG.F)
IMPIN6ER
TEMP
(OE6.F)
INLET OUTLET
920.
920.
520.
520.
920.
920.
920.
920.
920.
920.
520.
70.
72.
73.
75.
76.
76.
77.
77.
78.
78.
78.
70.
70.
70.
71.
71.
71.
71.
72.
73.
73.
73.
10.9
10.5
10.4
10.4
10.4
10.4
10.7
10.9
11.7
13.1
15.5
259.
2TO.
273.
270.
267.
268.
268.
266.
268.
270.
264.
•9.
«7.
•7.
48.
92.
92.
57.
93.
52.
52.
93.
TOTALS
AVERAGE
104.2
49.078
.72
.72 920.
79.
71.
11.4 268.
91.
-------
PARTICIPATE FIELD DATA * RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO/MP
TEST
8-5
COKE STACK
TEST DATE
ENGLISH UNITS
10/30/81
I
to
TB TIME-START
TF TIME-FINISH
TT NET TIME OF TEST, MIN,
NP NET SAMPLING POINTS
Y METER CALIBRATION FACTOR
ON SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY CAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL 1420 COLLECTED IN
IMPIN6ERS AND SILICA GEL,ML.
VNC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR MT-ORV STACK GAS
MMS MOLECULAR NT-STACK GAS
1623
104.2
11
1.033
.374 IN
.84
.72 IN-H20
49.078 CU-FT
METRIC UNITS
10/30/81
1439
1623
104.2
11
1.033
9.5 MM
.84
18.3 NM-M20
1.390 CU-M
73
SO
175
B
14
4
' 9
86
29
27
*
•
•
•
•
•
9
•
•
•
•
•
4 F
289 SCF
0
237 SCF
07
859
30
30
00
40
06
50
23.
1.
175.
•
14.
•
4.
9.
•
86.
29.
27.
0
424
0
233
07
859
30
30
00
40
06
50
C
SCM
SCM
-------
PB
PSI
PS
TS
VS
«s
OSSTD
03
ISO
MN
cs
PMR
•"
to
VD
BAROMETRIC PRESSURE
STATIC PRES OF STACK CAS
STACK PRES, AB8.
AVERA6E STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLON RATE, DRY*
ACTUAL STACK FLON RATE
PERCENT ISOKINETIC
FILTERABLE PART
M6. EPA S
FILTERABLE PART
FILTERABLE PART
EMISSION RATE
68 DIG F, 29.92 tN.Ht.
29.93 IN-H6
•1.20 IN-H20
29.84 IN-H6
S20. F
20.8 FPS
7466. SO-IN
1789295. SCFH
38751*8. ACFH
110.0
.0
.0000 GR/DSCF*
.000 L6/HR
760. ZZ 'MM-H6
•30.48 MM-H20
757.98 'HM-HG
271. C
6.3 NPS
4.817 SQ-M
50667. 3CHH
109733. ACMH
110.0
.0
.000 M6/D3CK
.00 KG/MR
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 6-5
STACK
VOLUME OF DDT CAS SAMPLED AT STANDARD CONDITIONS
VMSffi" • (17.447 i VM i Y * (PS » PM / 11.6)) / (TM * 460.)
17.647 * 49.078 • J.033 • ( 29.43 * .720 / 13.6)
VMSTD » — .— — i~ ......................................... • 90.289 D3CF
( 73. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC • .04707 • VLC
VHC •".04707 • 175. • ' T.'MTtF ~
PERCENT MOISTURE IN STACK CAS
~ BNO••r-(ioo. • VNCJ / (VMSTO * VNO
100. * 6.24
S, BHO • ——.———.—.—..... * 14.07 PERCENT
I 50.289 * 8.24
to
vo
MOLE FRACTION OF DRY STACK CAS
FMO • (100. • BNO) / 100.
100. - 14.1 - —
FMO « ——.......——...... • .859
100.
AVERCil MO\ECULAIT WEI6NT OF DRY STACK CIS
MO * (PC02 • .44) * (P02 • .32) * (PN2 * PCO) « .26
MO * (4.30*44/100) * ( 9.3*32/100) * ((86.0* .0) * 26/100 • 29.06
MOLECULAR WEIGHT OF STACK 6AS
MHS * MO * (1. - (BNO/100)) + 16. * (BNO/100)
MHS » 29.04* (1. -(14.07/100)1 » 18. • (14.07/100) * 27.50
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP • SUM. OF THE SORTtVM * (TS * 460.))
VS « 85.49 • CP • OELP / (SORT(MMS * PS) * PNTS)
VS • 85.49 * .84 * 91.108 / (SQRT( 27.50 • 29.84) • 11. a 20.76 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS • VS • AS • 3600/144
OS *~ 20.76 • 7466. 3600/144 * 3875168. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO i 17.6*7 • 68 • « * (17 i (BHO/IW) / (TS * 460.)
17.647 « 3875168. * 29,84 • (1. • (14.07/100))
OSSTO » ——.—————.—.——.-..———————« 1789295. SCFH
( 520. » 460.)
PERCENT ISOKINCTIC
<•> ISO » (305.58*(TS*460.))M(0.002669«VLC)«(VM«Yo(PB*(PM/l3.6))/(TM*46«.)))/(TT«VS«»PS»ON«DN)
*D
(SOS.58*( 520.**60.))•((«.00266t* 175.)*( 49.078«1.033*( 29.93»( .720/13.6))/C 73.4460.)))
ISO • ———————.————————[[[ • 110.00 PERCENT
104. * 20.76 * 29.84 « .374 • .374
PARTICIPATE LOADTN6 -- EPA METHOD 5 (AT »T*NOARD CONDITIONS)
CS = 0.001 • MN • 15.43 / VMSTD
CS * 0.001 • .0 * 15.43 / 50.289 « .000 GR/DSCF
PARTICIPATE LBS/HR — EPA METHOD 5
PMR » CS • OSSTO / (15*43 * 453.6)
-------
Run No. 8.5
Sample volume = 1.42 m3.50.29 scf
Example calculations
CS (Part) =183.6/1.42 =129.3 mq/m3
CS (Part) = 0.001 x183.6 x 15.43/50.29 =
3
CS (S02) = / = mg/m
= x 24.06/ = ppm
= 0.001 x x 15.43/.
gr/dscf
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 275°F
4-h at 275°F
2-h at 300°F
4-h at 300°F
2-h at 325°F
4-h at 325°F
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Sulfur dioxide
Sulfuric acid mist
As H2$04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
183.9
75.5
66.7
64.5
62.4
61.0
59.9
57.9
57.4
52.9
50.9
45.6
2 Concentration,
mg/m
129.5
53.2
47.0
45.4
43.9
43.0
42.2
40.8
40.4
37.2
35.8
32.1
gr/dscf
0.056
0.023
0.021
0.020
0.019
0.019
0.018
0.018
0.017
0.016
0.016
0.014
ppm
A-294
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(016.F)
BAR.PRESS.(IN.H6)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
COKE STACK
METHOD 8-600
DO/MP
47.
29.93
-1.20
3530214
97.90 .00
.84
..000 CFN 8 22.0 IN.H6
.982
DATE 10/30/81
RUN NUMBER 8-6
PROBE LENGTH • TYPE 4* QUARTZ
NOZZLE I 1.0. .620
ASSUMED MOISTURE 11.0
SAMPLE BOI NUMBER
METER BOX NUMBER FB8
METER HEAD DIFF. 1.91
C FACTOR .94
PROBE 'HEATER SETTING 290.
HEATER BOX SETTING 290.
REFERENCE PRESS. DIFF. .02
READ • RECORD DATA EVERY I0.i0 MINUTES
I
to
10
TRAVERSE
POINT
NO.
INIT
SAMPLE CLOCK
TIME TIME
(MIN.) (24-HR
^1 t\t*tt
(•LUC*
0 1*J«
10.0 1448
20.0 1498
30.
40.
50.
60.
to.
80.
1508
1518
1528
1938
1948
1998
90.0 1608
CAS METER
READING
(CU.FT.)
i
i
478.098
482.690
487.420
492.180
496.930
901.640
906.460
911.190
919.910
920.698
VELOCITY ORIFICE
PRESSURE
HEAD DIFFERENTIAL
(IN.H20) (IN.
DESIRED
. .._. ._
.070
.070
.070
.070
.070
.070
.070
.070
.070
.44
.44
.44
.44
.44
.44
.44
.44
.44
H20)
ACTUAL
.79
.79
.79
.79
.79
.79
.79
.75
.75
STACK
TEMP
(OE6.F)
520.
520.
520.
520.
520.
520.
520.
520.
520.
DRV CAB METER
TEMP
(DEG.P)
INLET OUTLET
67. 67.
69. 67.
72. 67.
73. 68.
75. 69.
75. 69.
75. 69.
74. 69.
75. 70.
PUMP
VACUUM
(IN.HG)
4.8
8.3
11.3
13.6
15.2
16.9
16.7
17.7
21.7
SAMPLE
BOX TEMP
(DEG.F)
984.
993.
601.
592.
601.
603.
599.
999.
600.
IMPINGER
TEMP
(DEG.F)
90.
46.
44.
48.
48.
90.
94.
94.
56.
TOTALS
AVERAGE
90.0
42.600
5.44
.75 520,
73.
68,
14.0 596.
;50.
-------
PARTICULATE FIELD DATA t RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND 00/MP
TEST
8-6
COKE STACK
TEST
TB
TF
TT
NP
Y
DN
CP
PM
DATE
f IME-ST ARf
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
ENGLISH UNITS
10/30/81
i«3e
1608
90.0
9
.982
.620 IN
.84
.75 IN-H20
METRIC UNITS
10/30/81
1438
1608
90.0
9
.982
15.7 MM
.84
19.1 MM-l
cn
DROP
VM VOLUME OF DRY CAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY CAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL M» "COLLECTED IN
IMPINCERS AND SILICA CELrNL.
VMC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
Blfb PERCENT MOISTURE 8V VOLUME
FMD MOLE FRACTION DRY CAS
PC02 PERCENT C02 BY VOL., DRY
P62 PCRCENT dZ BY VOL., 0«r
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR IT-DRY STACK CAS
MMS MOLECULAR NT-STACK CAS
42.600 CU-FT
1.206 CU-M
T0.6 F
41.722 SCF
isa.o
7.437 SCF
"15.11
.849
4.30
9.30
.00
86.40
29.06
27.39
21
1
158
15
4
9
86
29
27
.4 C
.181 8C*
.0
.211 SCX
.13
.849
.30
.30
.00
.40
.06
.39
-------
PB BAROMETRIC PRESSURE
PS! STATIC PRES Of STACK CAS
PS STACK PRES* ABS.
TS AVERAGE STACK TEMP
VS AVC STACK *A3 VELOCITY
AS STACK AREA
OSSTD STACK PLOW RATE. DRT*
OS ACTUAL ITAC* FLOW RATE
ISO PERCENT ISOKINETIC
MN FILTERABLE PART
MS. EPA 5
CS FILTERABLE PART
PMR FILTERABLE PART
EMISSION RATE
• 6ft C16 F, 2«.?MN.HG.
29.
-i<
29.
520.
20.
7466.
1771103.
3883105.
38.
•
.
.
93
20
84
*
IN-HG
IN-H20
IN-HG
F
FP8
SO-IN
B
0
0000
000
SCFH
ACFM
CR/D8CF*
LB/HR
760
-30
757
271
6
4
50152
109966
38
.22
.48
.98
•
.3
.817
•
•
.•
.0
.000
.00
MM-HG
•MM-H20
MM-HG
C
MP8
80-M
SCMH
ACMM
MG/D8CM
KG/MR
NJ
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 6-6
COKE STACK
VOLUME OF DRY 6AS SAMPLED AT STANDARD CONDITIONS
VMSTO « (17.647 * VM • T • (P8 * PM / IS.*)) / (TM * 460.)
17.647 • 42.600 • *982 • ( 29.93 * .750 / IS.6)
VMSTD • •——.—........................................... a 41.722 DSCF
( 71. » 460.)
VOLUME OP NATER VAPOR AT STANDARD CONDITIONS
VMC » .04707 • VLC
VNC * V01T07 • 158. » ~7ilt ICF
PERCENT MOISTURE IN STACK 6A8
BMOi~TiW. • VNC) / (VMSTO * VHC)
100. ft 7.44
> BNO « ———.—.——.——.— • 15.IS PERCENT
^ 41.722* 7.44
vo _
CO " "" --.—.._..
MOLE FRACTION OF DRV STACK 6AS
FMD • C100. - BNO) / 100.
FMO « ..........—.——— • .84*
100.
NE10HT OF ORV STACK SXB
MO • (PC02 • .44) • (P02 • .12) * (PN2 * PCO) • .28
MD « ( 4.30*44/100) * ( 9.S*S2/100) » ((8*. 4* .0) * 28/100 • 29.06
MOLECULAR NEI6MT OF STACK GAS
MNS * MO • (1. - (BNO/100)) * 18. • (BNO/ 100)
MMS « 29.06* (1. -(19.13/100)) • IS. • CIS. IS/100) • 27.39
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE SQRTtVH * (TS * 460,))
V8 * 85.49 • CP • OELP / (SORT(MM8 • PS) • PNTS)
VS » 85.49 • .84 • 74.543 / (SORT( 27.39 • 29.84) • 9. « 20.81 FPS
STACK 6AS VOLUMETRIC FLOW AT STACK CONDITIONS
OS * VS * AS • 3600/144
OS > 20.81 • 7466. 3*00/144 .• 3UI405. ACrM
STACK CAS VOLUMETRIC PLON AT STANDARD CONDITIONS
QSSTO • 17.647 * OS • «HT(IV- (BW07W)J / (TS « 460.)
17.647 * 38*3409. • 29.64 • (1. • (15.13/100))
OSSTD « ———————.———..................... • 1771103. 3CFH
( 520. * 460.)
PERCENT ISOKINETIC
ISO » (305.58*(TS*460.))*((0.002669*VLC) + (VM*Y*(MMPM/13.6))/(TMM6
(305.5«*( 520.4460.))•((0.002669* 156.J*( 42.600* .982*( 29.93*( .79f/13.6))/( 71.4460.)))
ISO « —«—...—.........—.-[[[ n 36.04 PERCENT
90. • 20.81 * 29.84 • .620 * .620
PARTICULAR LOADING -- IM METHOD S TAT1TAKOARO CONDITIONS)
CS » 0.001 * MN * 15.43 / VMSTO
C3 * 0.001 * .0 * 15.43 / 41.722 « .000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
-------
Run No. 8.6
Sample volume =_LJJLm ,_lLZ!scf
Example calculations
CS (Part) =45.1/1 ia e -?a 7 ma/m
CS (Part) = 0.001 x45.1 x 15.43/41.72= 0.017 qr/dscf
3
CS (S02) = / = mg/m
= x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Sulfur dioxide
Sulfuric acid mist
As H2S04
As H2S04-2H20
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
45.1
3 Concentration,
mg/m
38.2
gr/dscf
0.017
ppm
A-300
-------
2.0 DCOG Underfiring Test Series
December 1981
A-301
-------
FIELD 0»T*
o
to
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION NO.l COKE BATTERY OUTLET
SAMPLE TYPE PART/H2S04/S02
OPERATOR BRUFFEY
AMBIENT TEMP.(OEG.F) 3b.
BAR. PRESS. (IN. HG) 29.21
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530310
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .00
THERM. NO.
LEAKAGE .000 CFM 3 6.0 IN.HG
METER CALIB. FACTOR 1.003
READ » RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60. 0
70.0
80. 0
90.0
CLOCK
TIME
(24-HR
fi ftp K %
LLUtK J
1205
1215
1225
1235
1245
1255
1305
1315
1325
1335
GAS METER
READING
ICU.FT.)
259.553
263.720
260.400
273.200
277.960
202.600
207.420
292.730
296.060
301.507
VELOCITY
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.050
.050
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.67
.67
.67
.67
.67
.67
.67
.67
.67
H20)
ACTUAL
.67
.67
.67
.67
.67
.67
.67
.67
.67
STACK
TEMP
(DEG.F)
452.
463.
472.
467.
400.
492.
450.
459.
469.
DATE 12/00/81
RUN NUMBER 01-1
PROBE LENGTH * TYPE 4' HEATED GLASS
NOZZLE : I.D. .401
ASSUMED MOISTURE 14.0
SAMPLE BOX NUMBER 0
PETER BOX NUMBER FB2
METER HEAD OIFF. 1.00
C FACTOR .02
PROBE HEATER SETTING 250.
HEATER BUX SETTING 250.
REFENENCE PRESS. OIFF. .00
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
32. 32.
32. 33.
33. 32.
35. 32.
35. 32.
35. 33.
36. 33.
36. 33.
36. 33.
PUMP
VACUUM
(IN.HG)
4.0
4.0
4.0
4.0
5.0
6.0
5.5
6.0
6.0
SAMPLE
BOX TEMP
(DEG.F)
239.
255.
245.
240.
251.
243.
244.
241.
246.
IMPINGER
TEMP
(DEG.F)
34.
36.
36.
37.
36.
37.
39.
40.
40.
TOTALS
AVERAGE
90.0
42.034
.67
.67 460.
34.
33.
4.9 246.
37,
-------
PARTICIPATE FIELD DATA t RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST Dl-l
NO.l COKE BATTERY OUTLET
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
> PM
1
u>
o
U> VM
TM
VMSTD
VLC
VWC
BMO
FMD
PC02
P02
PCO
PN2
MO
MH3
TIME-START
TIME-FINISH
NET TIME OF TEST* MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL.* DRY
PERCENT 02 BY VOL.* DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR MT-DRY STACK GAS
MOLECULAR MT-STACK GAS
12/08/81
1205
1335
90.
9
1.
.
.
42.
33.
44.
103.
4.
9.
.
4.
9.
.
86.
29.
26.
0
003
401 IN
64
67 IN-H20
034 CU-FT
5 F
111 SCF
2
656 SCF
92
901
50
40
00
10
10
00
METRIC UNITS
12/06/61
1205
1335
90.0
9
1.003
10.2
.64
17.0
1.190
.6
1.249
103.2
.136
9.92
.901
4.50
9.40
.00
66.10
29.10
26.00
PM
PM-H20
CU-M
C
SCf
SCM
-------
PB
PSI
PS
TS
V3
AS
OSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE, DRY*
ACTUAL STACK FLON RATE
PERCENT ISOKINETIC
MG. EPA 5
EMISSION RATE
68 OEG f, 29.92 IN.H6.
29.21 IN-HG
-1.20 IN-H20
29.12 IN-HG
068. F
17.1 FPS
74bb. SO-IN
1595142. SCFH
3197639. ACFH
109.0
.0000
.00000 GR/DSCF*
.00000 LB/HR
7ai.93 CM-MG
-30.48 PM-H20
739.b9 MM-HG
242. C
5.2 CPS
4.817 SO-M
45170. SCKH
90548. ACHM
109.0
.0000
.0000 MG/OSCM
.000 KG/MR
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NU. 01-1
NO.l COKE BATTERY OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 • VM * Y • (P8 * PM / 13.6)) / (TM * 460.)
17.647 * 42.034 • 1.003 * ( 29.21 » .670 / 13.6)
VMSTO « —— = 44.111 DSCF
( 34. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC * .04707 * VLC
VNC * .04707 * 103. s 4.66 SCF
PERCENT MOISTURE IN STACK KAS
BNO » (100. * VNC) / fVMSTD » VHC)
^ 100. * 4.B6
f, BNO 3 —— — —- i 9.92 PERCENT
W 44.111 » 4.86
O
Ln
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - BNO) / 100.
100. • 9.9
FMO * ———— —— 3 .901
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MD a (PC02 * .44) * (P02 * .32) * (PN2 * PCO) * .28
MO * ( 4.50*44/100) » ( 9.4*32/100) » ((86.1* .0) * 26/100 = 29.10
MOLECULAR HEIGHT OF STACK GAS
MNS a MO • (1. • (BNO/100)) * 16. * (BNO/100)
MNS * 29.10* (1. -( 9.92/100)) * 18. * ( 9.92/100) 3 28.00
-------
STACK 6*3 VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SORUVH * (TS •» 460.))
VS • 65.49 • CP • OELP / (SORTlMKS * PS) * PNTS)
VS * 85.49 * .64 * 61.304 / (SORT( 86.00 * 29.12) * 9. = 17.13 FP3
STACK 8AS VOLUMETRIC FLO* AT STACK CONDITIONS
OS » VS * AS • 3600/144
OS a 17.13 * 7466. 3600/144 • 3197639. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO « 17.647 • OS » PS • (1. • (BNO/100)) / (TS + 460.)
17.647 » 3197639. * 29.12 *(!.-( 9.92/100))
OSSTD « — • = 1595142. SCFH
t 468. * 460.)
. PERCENT I30KINETIC
U) ISO B (305.56«(TS*460.))*((0.002669*VLC)«(VM*Y*(PB*(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN*ON)
O
^ (305.58*( 468.+460.))*((0.002669* 103.)*( 42.034*1.003*( 29.21*( .670/13.6))/( 34.4460.)))
ISO * — ............. . ... . .... . a 109.00 PERCENT
90. * 17.13 • 29.12 * .401 * .401
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS • 0.001 * MN * 15.43 / VMSTO
CS « 0.001 * .0000 * 15.43 / 44.111 = .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR « CS * OSSTD / (15.43 • 453.6)
PMR B .00000 * 1595142. / (15.43 * 453.6) = .00000
-------
Run No. D1.1
Sample volume = 1 .25 m r 44.11 scf
Example calculations
CS (Part) = 32.6/1.25 = 26.1 ma/m3
CS (Part) = 0.001 x 32.6 x 15.43/44.11 = 0.011 qr/dscf
3
CS (S02) = 69.7/1.25 = 55.8 mg/m
= 55.8 x 24.06/64 =21 ppm
= 0.001 x 69.7 x 1
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
32.6
21.8
21.1
16.8
16.4
14.6
0.0
0.0
<0.3
69.7
115*
N/A
N/A
N/A
3 Concentration,
mg/m
26.1
17.4
16.9
13.4
13.1
11.7
0.0
0.0
<0.2
55.8
92.0
gr/dscf
0.011
0.008
0.007
0.006
0.006
0.005
0.0
0.0
0.000
0.024
0.040
ppm
21
22
*Field analysis, isopropanol contaminated.
A-307
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(OEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COtFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
NO.I COKE BATTERY OUTLET
PART/H2S04/S02
BRUFFEY
36.
29.21
-1.20
3530320
97.50 .00
.84
.000 CFM 9
1.016
5.0 IN.HG
READ * RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
CLOCK)
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE STACK
DIFFERENTIAL TEPP
(IN.HZO) (DEG.F)
DATE
RUN NUMBER
PROBE LENGTH S TYPE
NOZZLE : 1.0.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
PETER BOX NUMBER
KETEH HEAD OIFF.
c FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS. DIFF,
12/08/01
Dl-i
5* HEATED GLASS
.401
14.0
0
FB5
1.86
.64
350.
850.
.00
DESIRED ACTUAL
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
PUHP SAMPLE
VACUUM BOX TEMP
(IN.HG) (OEG.F)
IMPINGER
TEMP
(OEG.F)
INIT
o
00
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
ao.o
90.0
1206
1216
1226
1238
1248
1258
1308
1318
1326
1338
TOTALS
AVERAGE
90.0
349.502
353.780
357.960
362.170
366.360
370.540
374.760
378.910
383.140
387.318
37.616
.050
.050
.050
.050
.050
.050
.050
.050
.050
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
.59
435,
465.
473.
471,
464.
495,
453.
462,
474.
466.
37.
36.
39.
40.
41.
43.
43.
43.
43.
41.
38.
30.
39.
39.
39.
40.
40.
4V.
40.
39.
2.0
2.0
2.0
2.0
3.0
2.0
2.5
2.0
2.0
269.
270.
273.
272.
270.
273.
275.
270.
279.
2.2 272.
33.
34.
36.
37.
36.
37.
35.
34.
30.
35.
-------
PARTICULATE FIELD DATA « RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFtY
TEST DI-Z
NO.l COKF. BATTERY OUTLET
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1
0 VM
VD
TM
VMSTD
VLC
VMC
BNO
FMD
PC02
P02
PCO
PN2
MD
HWS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-ORY STACK GAS
MOLECULAR MT-STACK GAS
ENGLISH UNITS
12/08/61
1206
1338
90.0
9
1.016
.401 IH
.64
.59 IN-H20
37.616 CU-FT
40.0 F
39.669 SCF
111.4
5.244 SCF
11.66
.663
4.50
9.40
.00
86.10
29.10
27.80
METRIC UNITS
12/08/61
1206
1338
90.0
9
1.016
10.2 VM
.84
15.0 PM-H20
1.071 CU-M
4.4 C
1.123 SCC
111.4
.146 SCM
11.66
.683
4.bO
9.40
.00
66.10
29.10
27.80
-------
PB
PSI
PS
TS
VS
AS
OSSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES* ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE» OR**
ACTUAL STACK FLOW RATE
PERCENT ISOKINEUC
MG. EPA 5
29.21 IN-HG
•1.20 IN-H20
29.12 IN-HG
468. F
IT.2 FPS
7466. SO-IN
1569507. SCFH
3206763. ACFH
99.6
.0000
.00000 GR/DSCF*
.00000 LB/HR
741.93 HM-HG
•30.46 KM-H20
739.69 PM-HG
242. C
5.2 fPS
4.617 SO-M
44444. SCMH
90863. ACPH
99.6
.0000
.0000 MG/OSCM
.000 KG/HR
EMISSION RATE
* 68 DEG F, 29.98 IN.HG.
U)
M
O
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. Dl-2
NO.I COKE BATTERY OUTLET
VOLUME OF ORT GAS SAMPLED AT STANDARD CONDITIONS
VMSTO • (17.647 • VM * Y • (PB + PM / 13.6)) / (TM » 460.)
17.647 • 37.816 • 1.016 * ( 39.21 «• .590 / 13.6)
VMSTD * — = 39.669 DSCF
( 40. •» 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC « .04707 • VLC
VNC » .04707 * 111. = 9.24 SCF
PERCENT MOISTURE IN STACK GAS
BMO * (100. * VNC) / (VMSTD * VHC)
100. • 5,24
BNO » — • —.... r M.68 PERCENT
39.669 » 5.24
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - BNO) / 100.
100. - 11.7
FMD « — ———— — » .883
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD * (PC02 * .44) * (P02 * .32) * (PN2 * PCO) • .28
MO = ( 4.50*44/100) «• ( 9.4*32/100) * ((86.1* .0) * 28/100 * 29.10
MOLECULAR HEIGHT OF STACK GAS
MHS * MD • (1. - (BHO/100)) » 18. * (BNO/100)
MHS * 29.10* (1. -(11.68/100)) * 18. * (11.68/100) s 27.80
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP • SUM. OF THE SORHVH * (TS » 060.))
VS a 85.49 • CP • DELP / (SORT(MWS • PS) * PNTS)
VS « 85.09 • .80 • 61.303 / (SORT( 27.80 * 29.12) * 9. = 17.19 FPS
STACK GAS VOLUMETRIC FLOM AT STACK CONDITIONS
OS « V3 • AS • 3600/100
OS * 17.19 • 7466. 3600/140 « 3208783. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD * 17.647 * OS * PS * (I. • (BHO/100)) / (TS * 460.)
17.647 * 3208783. * 29.12 * (1. • (11.68/100))
OSSTD * — — — ---- - --------------------- - ----------------- = 1569507. SCFH
( 468. » 460.)
PERCENT ISOKINETIC
ISO * (305.58*(TS+460.))*((0.002669*VLC)*(VM*Y*(PB»(PM/13.6))/(TM»460.)))/(TT*VS*PS*ON*DN)
(305.58*( 468. *460.))*((0. 002669* lll.)+( 37.816*1 .016* ( 29.21M .590/13.6) )/( O0.«460.)))
ISO » — — — ---- « — - ------- — --- ....... ---- .. ------- . ---------- - ------ ....... ----- ..... ------ . ----- - 99.62 PERCENT
90. * 17.19 * 29.12 * .401 • .001
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS « 0.001 • MN * 15.43 / VMSTD
C3 * 0.001 * .0000 * 15.43 / 39.669 = .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR a CS • OSSTD / (15.43 • 453.6)
PMR • .00000 * 1569507. / (15.43 * 453.6) = .00000
-------
Run No. PL2
Sample volume = 1.12 m r 39.67
Example calculations
CS (Part) = 37.4/1.12 = 33.4 mq/m3
CS (Part) = 0.001 x 37.4 x 15.437 39.67= Q.Q14 qr/dscf
CS (S02) =116.1/1.12 = 103.7ma/m3
= 103.7X 24.06/64 = 39 ppm
= 0.001 x 116.1X 15.43/39.67 == 0.045 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
37.4
22.0
2.0
2.7
2.1
116.1
3.5
N/A
N/A
N/A
3 Concentration,
mg/m
33.4
19.6
1.8
2.4
1.9
103.7
3.1
gr/dscf
0.014
0.008
0.001
0.001
0.001
0.045
0.001
ppm
39
1
A-313
-------
FIELD DAT*
I
U)
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET
SAMPLE TYPE PART/H2304/S02
OPERATOR DAN FITZGERALD
AMBIENT TEMP. (DEC. F) 36.
BAR. PRESS. (IN. HG) 29.21
STATIC PRESS. ( IN. H20) -1.20
FILTER NUMBER(S) 3530349
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .84
THERM. NO. 133
LEAKAGE .012 CFM 9 5.
METER CALIB. FACTOR 1.031
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INtT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
SO.O
60.0
70.0
60. 0
90.0
CLOCK
TIME
(Z4-HR
^i nr v \
CLUCK!
1205
1215
1225
1235
1245
1255
1305
1315
1325
1335
GAS METER
READING
(CU.FT.)
US. 363
169.785
174.100
176.120
182.375
186.670
190.950
195.325
199.630
203.870
VELOCITY
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.050
.050
CLEVELAND OHIO
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.66
.66
.65
.66
.6«
.64
.66
.66
.65
H20)
ACTUAL
.66
.66
.65
.66
.64
.64
.66
.66
.65
STACK
TEMP
(DEG.F)
452.
463.
472.
467.
488.
492.
450.
459.
470.
DATE 12/08/81
RUN NUMBER 01-3
PROBE LENGTH S TYPE 4 FOOT GLASS
NOZZLE 1-3 t I.D. .402
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
METER BOX NUMBER FBI
METER HEAD DIFF. i.ee
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
K FACTOR 12094.5
DRY GAS METER
TEMP
(OEG.F)
INLET OUTLET
37. 37.
38. 37.
41. 38.
43. 38.
45. 38.
46. 39.
47. 40.
47. 40.
47. 40.
PUMP
VACUUM
(IN.HG)
1.0
1.0
1.0
2.0
3.0
3.5
3.5
4.0
4.5
SAMPLE
BOX TEMP
(DEG.F)
381.
373.
378.
375.
373.
369.
370.
372.
372.
IMPINGER
TEMP
(OEG.F)
38.
39.
43.
44.
46.
47.
50.
52.
54.
TOTALS
AVERAGE
90.0
38.507
.65
.65 468.
43.
39,
2.6 374.
46.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST Dl-3
STACK OUTLET
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1 VM
u>
I-1
en
TM
VMSTD
VLC
VMC
BMO
FMD
PCOZ
POZ
PCO
PNZ
MD
HW3
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL HZO COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF WATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
12/08/81
1205
1335
90.0
9
1.033
.402 IN
.84
.65 IN-H20
38.507 CU-FT
41.0 F
40.994 SCF
113.9
5.361 SCF
11.57
.884
4.50
9.40 .
.00
86.10
29.10
27.81
METRIC UNITS
12/08/81
1205
1335
90.0
9
1.033
10.2
.84
16.6
1.090
5.0
1.161
113.9
.152
11.57
.884
4.50
9.40
.00
86.10
29.10
27.81
I'M
PM-H20
CU-M
C
SCM
SCM
-------
PB
PSI
PS
TS
VS
»3
OS3TD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK CAS VELOCITY
STACK AREA
STACK FLO* RATE, DRY*
ACTUAL STACK FLON RATE
PERCENT ISOKINETIC
MG. EPA 5
EMISSION RATE
66 DEC f, 29.42 IN.HG.
29.21 IM-HG
-1.20 IN-H20
29.12 IN-HG
468. F
17.2 FPS
7505. SO-IN
1579103. SCFH
3224786. ACFH
102.3
.0000
.00000 GR/OSCF*
.00000 L8/HR
741.93 HM-HG
•30.48 WN-H20
739.69 *M-HG
242. C
5.2 WPS
4.842 30-M
44715. SC*H
91316. ACHH
102.3
.0000
.0000 MG/DSCM
.000 KG/HR
>
co
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 01-3
STACK OUTLET
VOLUME OF DRY 6*3 SAMPLED AT STANDARD CONDITIONS
VMSTO » (17.647 • VM • Y * (PB * PM / 13.6)) / (TM » 460.)
17,647 • 38.507 * 1.033 * ( 29.31 * .653 / 13.6)
VMSTD » ——————.—.———— — — — — — = 40.994 DSCF
( 41. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC * .04707 • VLC
VNC « .04707 * 114. a 9.36 SCF
PERCENT MOISTURE IN STACK GAS
BMO a (100. • VHC) / (VMSTD • VNC)
> 100. • 5.36
' BNO * ———— ...—.. s 11.57 PERCENT
i_. 40.994 » 5.36
MOLE FRACTION OF DRY STACK GAS
FMD • (100. • BMO) / 100.
100. • 11.6
FMD a —• —— ....... * .864
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD a (PC02 * .44) * (P02 • .32) * (PN2 * PCO) • .28
MD • ( 4.50*44/100) » ( 9.4*32/100) * ((86.1* .0) * 26/100 = 29.10
MOLECULAR HEIGHT OF STACK GAS
MH9 a MD * (1. • (BNO/100)) + 18. * (BMO/100)
MNS • 29.10* (1. -(11.57/100)) * 18. • (11.57/100) a 27.81
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP « SUM. OF THE SQRUVH * (TS * 060.))
VS * 85.49 * CP • DELP / (SORT (MWS * PS) * PNTS)
VS * SS.49 * .84 • 61.308 / (3QRT( 37.81 * 29.13) * 9. = 17.19 FPS
STACK 6A3 VOLUMETRIC FLOW AT STACK CONDITIONS
OS * VS * AS • 3600/144
OS * 17.19 t 7505. 3600/144 * 3224786. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
8SSTD » 17.647 * OS * PS * (1. - (BwO/100)) / (TS * 460.)
17.647 * 3224786. * 29.12 * (1. - (11.57/100))
OSSTO « — ——— • = 1579103. SCFH
( 468. * 460.)
> PERCENT ISOKINETIC
£ ISO * (305.58*(TS+460.))*((0.002669*VLC)»(VM*Y*(PB«(PM/13.6))/(TM+460.)))/ITT*VS*PS*DN*ON)
00
(305.58*( 468.+460.))*((0.002669* 114.)*( 38.507*1.033*1 29.21+1 .653/13.6))/( 41.«460.)))
ISO * —————— . — ...... ................ . — s 102.34 PERCENT
90. * 17.19 * 29.12 * .402 * .402
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTO
CS s 0.001 * .0000 * 15.43 / 40.994 s .00000 GR/OSCF
PARTICULATE LBS/HR ~ EPA METHOD 5
PMR * CS * OSSTD / (15.43 * 453.6)
PMR s .00000 * 1579103. / (15.43 * 453.6) s .00000
-------
Run No. PI.3
3
Sample volume = 1.16 m T 40.99 scf
Example calculations
CS (Part) =34.0/1.16 = 29.3 mq/m3
CS (Part) = 0.001 x34.0 x 15.43^0.99 = 0.013 qr/dscf
CS (S02) =117.0/1.16 =100.9ma/m3
= 100.9x 24.0664 =38 ppm
= 0.001 xlU.Ox 15.43/_4_OJ2_=0_J}4J_ gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S0d=
Sulfur dioxide
Sulfuric acid mist
As H2$04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
34.0
0.0
0.0
2.5
117.0
9.3
N/A
N/A
N/A
3 Concentration,
mg/m
29.3
0.0
0.0
2.1
100.9
8.0
gr/dscf
0.013
0.000
0.000
0.001
0.044
0.004
ppm
38
2
A-319
-------
FIELD DATA
U)
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET «1
SAMPLE TYPE PART/H2S04/S02
OPERATOR DAN FITZGERALD
AMBIENT TEMP. (DEC. F) 36.
BAR. PRESS. UN. KG) 2V. 21
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530363
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .04
THERM. NO. 133
LEAKAGE .001 CFM 9 5.
METER CALIB. FACTOR .902
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
ao.o
90.0
CLOCK
TIME
(20-HR
f* i nf k i
CLUCK]
1208
1210
1220
1230
1240
1250
1300
1310
1320
1330
GAS METER
READING
(CU.FT.)
597.103
601.255
605.610
610.030
614.360
616.650
622.940
627.325
631.705
636.074
VELOCITY
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.050
.050
CLEVELAND OHIO
8ATTEHY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.66
.66
.65
.66
.64
.63
.66
.66
.65
H20)
ACTUAL
.66
.66
.65
.66
.64
.63
.66
.66
.65
STACK
TEMP
(DEG.F)
055.
465.
473.
471.
404.
495.
453.
462.
474.
DATE 12/00/01
NUN NUMBER 01-4
PROBE LENGTH « TYPE 5 FOOT GLASS
N02ZLE 1*4 : I.I). .401
ASSUMED MOISTURE 13.7
SAMPLE BUX NUMBER
PETER BUX NUMBER FBS
HETER HEAD OIFF. 1.91
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
K FACTOR 12094.5
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
36. 34.
30. 32.
40. 35.
42. 36.
44. 36.
44. 36.
45. 37.
45. 37.
45. 37.
PUMP
VACUUM
(IN.HG)
1.5
1.5
1.5
1.5
2.5
3.0
3.5
3.5
3.5
SAMPLE
BOX TEMP
(DEG.F)
304.
332.
341.
339.
330.
330.
335.
334.
343.
IMPINGER
TEMP
(DEG.F)
40.
42.
40.
40.
42.
43.
44.
46.
47.
TOTALS
AVERAGE
90.0
30.971
.65
.65 470,
42.
36.
2.4 333.
43.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST 01-0
STACK OUTLET »1 BATTERY
TEST DATE
TB
TF
TT
NP
T
ON
CP
PM
fr
1
U) VM
KJ
M
TM
VMSTO
VLC
VNC
BNO
FMO
PC02
P02
PCO
PN2
MO
MHS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRV
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR MT-DRV STACK GAS
MOLECULAR XT-STACK GAS
ENGLISH UNITS
12/08/61
1208
1336
90.0
9
.982
.401 IN
.84
.65 IN-H20
38.971 CU-FT
38.8 F
39.611 SCF
103.5
4.872 SCF
10.95
.890
4.50
9.40
.00
86.10
29.10
27.88
METRIC UNITS
12/08/81
1208
1338
90.0
9
.982
10.2 MM
.84
16.6 PM-H20
1.104 CU-M
3.8 C
1.122 SCM
103.5
.138 SO
10.95
.890
4.50
9.40
.00
86.10
29.10
27.88
-------
PB
Pdl
PS
TS
VS
AS
QSSTD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRESf ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK PLON RATE* DRY*
ACTUAL STACK FLO* RATE
PERCENT ISOKINETIC
M6. EPA 5
EMISSION RATE
68 OEG F, 39.92 IN.HG.
29.81 IN-HG
•1.20 IN-H20
29.12 IN-HG
470. F
17.2 FPS
7505. SQ-IN
1586320. SCFH
3224520. ACFH
98.9
.0000
.00000 GR/DSCF*
.00000 LB/HR
741.93 CM-HG
-30.48 PM-H20
739.69 MM-MG
243. C
5.2 VPS
4.842 3Q-M
44920. SCKH
91309. ACMH
98.9
.0000
.0000 MG/DSCM
.000 KG/HR
U)
to
N)
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. Dl-4
STACK OUTLET HI BATTERY
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VM9TD • (17.647 • VM • Y * (PB * PM / 13.6)) / (TM » 460.)
17.647 • 38.971 • .982 * ( 29.21 * .652 / 13.6)
VMSTO « —————............ .......................— 5 39.611 DSCF
( 39. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VNC « .04707 * VLC
VNC • .04707 « 104. = 4.87 SCF
PERCENT MOISTURE IN STACK GAS
BNO » (tOO. * VNC) / (VMSTD * VNC)
100. * 4.87
BNO » ——— — — r 10.95 PERCENT
39.611 » 4.87
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - BNO) / 100.
100. • 11.0
FMD • ————— B .890
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD * (PC02 * .44) * (P02 • .32) * (PN2 * PCO) * .28
MO « ( 4.50*44/100) * ( 9.4*32/100) * ((86.1* .0) * 28/100 = 29.10
MOLECULAR NEIGHT OF STACK GAS
MNS • MD * (1. - (8*0/100)) * 18. * (8*0/100)
MNS « 29.10* (1. -(10.95/100)) * 18. * (10.95/100) • 27.88
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SQRHVH * (TS * 060.))
VS * BS.49 * CP * DELP / (SORT(MWS * PS) • PNTS)
VS » 65.49 * .84 * 61.378 / (SORTl 27.88 * 29.12) * 9. c 17.19 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS • 17.19 • 7SOS. 3600/144 a 3224520. ACFH
STACK GAS VOLUMETRIC FLOH AT STANDARD CONDITIONS
098TD * 17.647 * OS * PS * (1. - (BNO/100)) / (TS * 460.)
17.647 • 3224520. * 29.12 * (1. - (10.95/100))
OSSTO » ———— —— = 1586320. SCFH
( 470. * 460.)
•f PERCENT ISOKINETIC
U)
N) ISO * (305.58*ITS*460.))*((0.002669*VLC)*(VM*Y*(PB*(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN*DN)
it»
(305.58*( 470.+460.))*((0.002669* 104.)*( 38.971* .982*( 29.21*( .652/13.6))/( 39.«460.)))
ISO » ————— ....... . ....... . ................ ..... s 98.93 PERCENT
90. * 17.19 * 29.12 * .401 * .401
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS « 0.001 • MN • 15.43 / VMSTD
CS * 0.001 * .0000 * 15.43 / 39.611 c .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR » CS • OSSTD / (15.43 • 453.6)
PMR * .00000 * 1586320. / (15.43 * 453.6) = .00000
-------
Run No. D1.4
o
Sample volume = 1.12m ,39.61 scf
Example calculations
CS (Part) = 43.3/1.12 = 38.7 mq/m3
CS (Part) = 0.001 x 43.3 x 15.43/39.61 = 0.017 qr/dscf
CS (S02) =115.8/1.12 = 103.4ma/m3
=103.4 x 24.06/64 = 39 pom
= 0.001 x115.8 x 15.43/39.61 = 0.045 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04-
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
43.3
•
0.0
0.0
0.0
115.8
9.2
N/A
N/A
N/A
3 Concentration,
mg/m
38.7
0.0
0.0
0.0
103.4
8.2
gr/dscf
0.017
0.000
0.000
0.000
0.045
0.004
ppm
39
2
A-325
-------
FIELD DAT*
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
COKE STACK
MB-600
OU
37.
29.21
-1.20
3530220
97.50 .00
.83
.012 CFM a
.967
8.0 IN.HG
READ I RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE CLOCK
TIME TIME
(MIN.) (24-HR
CLOCK)
GAS METER
READING
ICU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE STACK
DIFFERENTIAL TEMP
(IN.H20) (DEG.F)
DATE 12/08/81
RUN NUMBER 01-6
PROBk LENGTH ft TYPE 6* GLASS
NOZZLE : I.U. .379
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
METE* BOX NUMBER FB6
METER HEAD OIFF. 1.51
C FACTOR .71
PROBE HEATER SETTING 6UU.
HEATER BOX SETTING 600.
REFERENCE PRESS. DIFF. .22
DRY GAS METER PUMP
TEMP VACUUM
(DtG.F) (IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPINGER
TEMP
(DEG.F)
DESIRED ACTUAL
INLET OUTLET
INIT
UJ
fO
TOTALS
AVERAGE
0
10.0
20.0
30.0
40.0
SO.O
60.0
70.0
80.0
90.0
90.0
1209
1219
1229
1239
1249
1259
1309
1319
1329
1339
646.852
650.750
654.450
658.220
661.860
665.690
669.490
673.300
677.120
680.811
33.959
.040
.040
.040
.040
.040
.040
.040
.040
.040
.35
.35
.35
.35
.35
.35
.35
.35
.35
.35
.35 485.
.35 485.
.35 485.
.35 405.
.35 485.
.35 485.
.35 485.
.35 485.
.35 485.
.35 485.
34,
35,
36,
39.
40.
41.
41.
42.
42.
39,
37,
37,
37.
37.
37,
37,
37.
37,
37,
37,
3.2
3.0
3.0
3.2
4.0
6.0
6.5
6.8
7.1
569.
573.
510.
447.
489.
486.
514.
516.
529.
4.8 515.
34.
34.
33.
33.
33.
34.
33.
34.
34.
34.
-------
PARTICIPATE FIELD DATA t RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND 00
TEST 01-6
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1
OJ VM
N)
-J
TM
VMSTD
VLC
VMC
BNO
FMD
PC02
P02
PCO
PN2
MD
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
12/08/81
1209
1339
90.0
9
.967
.379 IN
.63
.35 IN-H20
33.959 CU-FT
37.9 F
34.024 SCF
81.8
3.850 SCF
10.17
.898
4.50
9.40
.00
86.10
29.10
27.97
METRIC UNITS
12/08/81
1209
1339
90.0
9
.967
9.6
.83
8.9
.962
3.3
.963
81.8
.109
10.17
.896
4.50
9.40
.00
86.10
29.10
27.97
MM
MM-H20
CU-M
C
SO
SCM
-------
PB
PSI
PS
TS
V3
AS
OSSTD
OS
ISO
HN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, A8S.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE* DRY*
ACTUAL STACK FLON RATE
PERCENT ISOKINETIC
MG. EPA 5
29.21 IN-HG
-1.20 IN-H20
29.12 IN-Ht
485. F
15.3 FPS
7466. 30-IN
1393914. SCFH
2653244. ACFH
107.7
.0000
.00000 GR/OSCF*
.00000 LB/HK
EMISSION RATE
* 68 DEC f, 29.93 IN.HG.
741.93 KM-HG
-30.48 CM-H20
739.69 CM-HG
252. C
4.7 MPS
4.817 SO-M
39471. SCMH
80795. ACHH
107.7
.0000
.0000 MG/OSCM
.000 KG/HR
00
-------
to
vo
EXAMPLE PARTICULATE CALCULATIONS TEST NO. Dl-6
COKE STACK
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 • VM • V • (PB * PM / 13.6)) / (TM + 460.)
17.647 • 33.959 * .967 * ( 29.21 * .350 / 13.6)
VMSTD * ———— — — ......................... ....... c 34.024 DSCF
( 38. * 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VNC • .04707 • VLC
VNC « .04707 * 82. > 3.65 SCF
PERCENT MOISTURE IN STACK GAS
BNO » (100. • VMC) / (VMSTD * VNC)
100. • 3.85
BNO * ———. .. .. — r 10.17 PERCENT
34.024 * 3.85
MOLE FRACTION UF DRV STACK GAS
FMD « (100. - BNO) / 100.
100. • 10.2
FMD « ———-.— ....... m .698
100.
AVERAGE MOLECULAR HEIGHT OF DRV STACK GAS
MD « (PC02 • .44) * (P02 * .32) * (PN2 » PCO) * .28
MD e C 4.50*44/100) «• ( 9.4*32/100) » ((86.1* .0) * 28/100 = 29.10
MOLECULAR HEIGHT OF STACK GAS
MNS * MD • (1. • (BHO/100)) * 18. * (BNO/100)
MNS » 29.10* (1. -(10.17/100)) * IB. * (10.17/100) « 27.97
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP * SUM. OF THE SORTtVH * (TS * 460.))
VS * 85.49 * CP * OELP / (SORT(MNS * PS) * PNTS)
V3 » 85.49 * .83 * 55.334 / (SORT( 27.97 * 29.12) * 9. r 15.29 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS « VS * A3 * 3600/144
OS » 15.29 * 7466. 3600/144 » 2853244. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTO • 17.647 * OS * PS * (t. - (BWO/100)) / (TS « 460.)
17.647 • 2853244. * 29.12 * (1. • (10.17/100))
OSSTO » —————— ... ... .. s 1393914. SCFH
I 485. * 460.)
PERCENT ISOKINETIC
ISO « (305.58*(T8*460.))*((0.002669*VLC)*(VM*Y*(PBMPM/13.6))/(TM.i460.)))/(TT*VS*PS*DN*DN)
(305.58*( 485.»460.})*((0.002669* 82.)*( 33.959* .967*( 29.21M .350/13.6))/( 38.«460.)H
ISO » .-.—.—...... . ....... . . ... s 107.70 PERCENT
90. * 15.29 * 29.12 * .379 * .379
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS • 0.001 • MN * 15.43 / VMSTO
CS * 0.001 * .0000 * 15.43 / 34.024 a .00000 GR/DSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR » CS * QSSTD / (15.43 * 453.6)
PMR * .00000 * 1393914. / (15.43 * 453.6) « .00000
-------
Run No. PI.6
Sample volume =0.96 m3.34.02 scf
Example calculations
CS (Part) =27.3 /0.96 = 28.4 mq/m3
CS (Part) = 0.001 x 27.3 x 15.43/34.02 = 0.012 qr/dscf
CS (S02) = 97.9/0.96 =102.0 mq/m3
=102.0 x 24.06/64 = 38 ppm
= 0.001 x 97.9 x 15.43/34.02 = Q.Q44 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
27.3
0.0
0.0
1.6
97.9
6.3
N/A
N/A
N/A
- Concentration,
mg/m
28.4
0.0
0.0
1.7
102.0
6.6
gr/dscf
0.012
0.0
0.0
0.001
0.044
0.003
ppm
38
2
A-331
-------
FIELD I)»T»
to
u>
tO
PLANT REPUBLIC STEEL
SAMPLING LOCATION OUTLET STACK
SAMPLE TYPE PART/H2S04/S02
OPERATOR BRUFFEY
AMBIENT TEMP. (DEG.F) 28.
BAR. PRESS. (IN.HG) 29.51
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530310
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM a 6.
METER CALIB. FACTOR 1.003
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT
NO.
1NIT
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
TIME
(24-HR
ft flf* H \
ILUIK J
1341
1351
1401
1411
1421
1431
1441
1451
1501
1511
READING
(CU.FT.)
312.901
317.610
323.165
328.267
333.390
338.747
343.910
349.160
354.465
359.464
HEAD
(IN.H20)
.060
.065
.064
.066
.066
.060
.064
.064
.060
CLEVELAND
0 IN.HG
ORIFICE PRESSURE
STACK
DIFFERENTIAL TEPP
(IN.
DESIRED
.79
.86
.64
.87
.90
.79
.84
.84
.79
H2U)
ACTUAL
.79
.86
.84
.87
.90
.79
.84
.84
.79
(DEG.F)
500.
491.
505.
465.
476.
491.
473.
488.
496.
DATE 12/10/81
RUN NUMBER 02-1
PROBE LENGTH R TYPE 5' HEATfcl) GLASS
NOZZLE : I.D. .404
ASSUMED MOISTURE 14.0
SAMPLE BOX NUMBER 0
PETErt BOX NUMBER FB2
PETER HEAD DIFF. i.76
C FACTOR .62
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. OIFF. .14
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP
(DEG
INLET
35.
35.
36.
37.
37.
37.
39.
38.
36.
.F)
OUTLET
32.
30.
30.
30.
30.
30.
30.
30.
30.
VACUUM
(IN.HG)
3.0
3.0
3.0
3.5
5.0
5.5
5.8
6.0
6.0
BOX TEMP
(DEG.F)
180.
236.
245.
234.
253.
254.
260.
262.
273.
TEMP
(DEG.F)
34.
36.
40.
37.
36.
38.
42.
42.
42,
TOTALS
AVERAGE
90.0
46.583
.84
.64 487.
37,
30.
4.5 244.
39.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BHUFFEY
TEST 08-1
OUTLET STACK
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
> PM
U)
LO
to VM
TM
VM3TD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
12/10/81
1341
1511
90
9
1
46
33
49
.0
.003
.404 IN
.84
.84 IN-H20
.583 CU-FT
.6 F
.401 SCF
METRIC UNITS
12/10/81
1341
1511
90
9
1
10
21
1
1
.0
.003
.3
.84
.2
.319
.9
.399
MM
MM-H20
CU-M
C
SCM
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VMC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BMO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRV
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR HT-ORY STACK GAS
MhS MOLECULAR NT-STACK GAS
145.9
6.868 SCF
145.9
.194 SCC
12.20
.878
4.30
12.30
.00
83.40
29.18
27.82
12.20
.878
4.30
12.30
.00
83.40
29.18
27.82
-------
PB
PSI
PS
TS
VS
AS
QS9TD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRE9 OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE, DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
29.51 1N-MG
•1.20 1N-M20
29.02 IN-HG
087. F
FPS
SO-IN
SCFH
ACFH
19.5
7466.
1707391.
3631009.
109.6
.0000
.00000 GR/OSCF*
.00000 LB/HR
709.55 MM-HG
•30.08 KM-H20
707.31 KM-HG
253. C
5.9 UPS
0.817 SO-M
09081. SCMH
102820. ACMH
109.8
.0000
.0000 MG/DSCM
.000 KG/HR
EMISSION RATE
* 68 DEC f, 29.92 IN.HG.
U)
UJ
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 02-1
OUTLET STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO « (17.647 • VM * V • (PB •» PM / 13.6)) / (TM + 460.)
17.647 * 46.563 * 1.003 • ( 29.51 * .636 / 13.6)
VMSTD » ———— • = 19.401 DSCF
( 34. + 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC * .04707 * VLC
VMC • .04707 * 146. = 6.67 SCF
PERCENT MOISTURE IN STACK GAS
BNO » (100. • VMC) / (VMSTO + VNC)
100. * 6.67
BNO « ..———.-.............. 3 12.20 PERCENT
> 49.401 * 6.67
UJ-
U)
en
MOLE FRACTION OF DRY STACK GAS
FMO » (100. • BHO) / 100.
100. - 12.2
FMD • ———— —— • .878
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD » (PC02 * .44) * (P02 * .32) * (PN2 « PCO) • .26
MO * ( 4.30*44/100) » (12.3*32/100) » ((83.0+ .0) • 26/100 x 29.18
MOLECULAR HEIGHT OF STACK GAS
MfcS a MD • (1. • (BHO/100)) + 18. * (BMO/100)
MN9 » 29.16* (1. -(12.20/100)) 4 16. * (12.20/100) * 27.62
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP « SUM. OF THE SORT(VH * (TS •» 460.))
V3 a 85.49 * CP * OELP / (SQRT(MNS * PS) * PNTS)
VS = 85.49 • .84 • 69.746 / (SORT( 27.82 • 29.42) • 9. = 19.45 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS a VS * AS • 3600/144
OS * 19.45 • 7466. 3600/144 * 3631049. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO * 17.647 * OS * PS * (1. » (BMO/100)) / (TS * 460.)
17.647 * 3631049. * 29.42 * (1. • (12.20/100))
OSSTO « — • — • s 1747391. SCFH
( 487. + 460.)
>
I PERCENT ISOKINETIC
OJ
J£ ISO • (305.58*(T3+460.))*((0.002669*VLC)*(VM*T*(PB«(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN*DN)
(305.58*( 487.«460.))*((0.002669* 146. )*( 46.583*1.003* ( 29.51*( .836/13.6))/( 34.«460.)))
ISO » ————— —— — ...... . . ... ... .... . .. s 109.78 PERCENT
90. * 19.45 * 29.42 « .404 * .404
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS » 0.001 • MN * 15.43 / VMSTO
CS * 0.001 * .0000 * 15.43 / 49.401 > .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR • CS * OSSTD / 115.43 « 453.6)
PMR * .00000 * 1747391. / (15.43 * 453.6) • .00000
-------
Run No. D2.1
Sample volume = 1.40 m3. 49.40 scf
Example calculations
CS (Part) =249.9/ 1.40=178.5 mq/m3
CS (Part) = 0.001 X249.9X 15.43/49.40= 0.078 qr/dscf
CS (S02) = 120.&/ 1.40=86.3 mq/m3
= 86.3 x 24.067 64 =32 ppm
= 0.001 x 120.8X 15.43/49.4 = 0.038gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
249. 9a
1.0
1.4
0.9
120.8
13.7
N/A
N/A
N/A
, Concentration,
mg/m
178.5
0.7
1.0
0.6
86.3
9.8
gr/dscf
0.078
0.0003
0.0004
0.0003
0.038
0.004
ppm
32
2
Acetone rinse contaminated with oil
-------
FIELD DATA
CO
OJ
CO
PLANT REPUBLIC STEEL CLEVELAND
SAMPLING LOCATION OUTLET STACK
SAMPLE TYPE PART/H2S04/S02
OPERATOR 8RUFFEY
AMBIENT TEMP. (DEG.F) 28.
BAR. PRESS. (IN. MS) 29.51
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBEH(S) 3530050
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .000 CFM 9 5.0 IN.HG
METER CALIB. FACTOR 1.004
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY ORIFICE PRESSURE STACK
POINT TIME TIME READING MEAD DIFFERENTIAL TEMP
NO. (MIN.J (24-HR ICU.FT.) (IN.H20) (IN.H20) (DEG.F)
INIT 0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
\>uu\«™ /
1308
1318
1328
1338
1348
1358
1408
1418
1428
1438
1448
1458
1508
DESIRED
423.038
427.790
433.075
438.330
443.500
448.300
452.740
457.880
463.160
468.020
473.010
478.050
482.903
.060
.067
.068
.061
.065
.064
.066
.068
.060
.064
.064
.061
.73
.88
.90
.74
.70
.80
.85
.89
.73
.80
.80
.74
ACTUAL
.73
.88
.90
.74
.70
.80
.85
.09
.73
.80
.80
.74
DATE 12/10/81
RUN NUMBER 02-2
PROBE LENGTH ft TYPE 4' HEATED GLASS
NOZZLE : 1.0. .4UO
ASSUMED MOISTURE 14.0
SAMPLE BOX NUMBER 0
METER BOX NUMBER FBI
METER HEAD DIFF. 1.71
C FACTOR .84
PRUBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .14
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM BOX TEMP TEMP
(DEG.F) (IN.HG) (OEG.F) (DEG.F)
INLET OUTLET
500.
481.
489.
478.
491.
505.
465.
476.
491.
173.
488.
496.
39.
03.
46.
46.
46.
46.
46.
46.
46.
47.
46.
46.
35.
36.
36.
36.
35.
35.
35.
36.
36.
36.
35.
35.
1.5
2.0
2.0
2.U
2.0
3.0
3.0
3.5
4.0
4.0
4.5
4.5
223.
200.
210.
199.
220.
232.
218.
230.
240.
246.
252.
265.
35.
36.
38.
39.
37.
40.
34.
35.
36.
40.
40.
40.
TOTALS
AVERAGE
120.0
59.865
.80
.80 486.
45,
36.
3.0 229.
38.
-------
PARTICIPATE FIELD DATA a RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BHUFFEY
TEST DZ-Z
OUTLET STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
W V"
^P
TM
VMSTD
VLC
VNC
BNO
FMD
PC02
POZ
PCO
PNZ
MD
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL HZO COLLECTED IN
IMPIN6ERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT NZ BY VOL., DRY
MOLECULAR HT-ORY STACK GAS
MOLECULAR MT-STACK GAS
ENGLISH UNITS
12/10/61
1308
1508
120.0
12
1.004
.400 IN
.84
.80 IN-HZO
59.865 CU-FT
40.4 F
62.678 SCF
181.9
8.562 SCF
12.02
.880
4.30
12.30
.00
83.40
29.18
27.84
METRIC UNITS
12/10/81
1308
1508
120.0
12
1.004
10.2 MM
.84
20.2 PM-HZO
1.695 CU-M
4.7 C
1.775 SCM
181.9
.242 SCC
12.02
.880
4.30
12.30
.00
83.40
29.18
27.84
-------
PB
PSI
PS
TS
VS
AS
033TO
OS
ISO
UN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE* DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
M6. EPA 5
EMISSION RATE
DEG f, 29.92 IN.HG.
29. 51 IN-HG
-1.20 IN-H20
29.42 IN-HG
466. F
19.5 FPS
74bb. SO-IN
1759182. SCFH
3643425. ACFH
105.9
.0000
.00000 GR/DSCF*
.00000 LB/HR
749.55 f»M-HG
-30.48 *M-H20
747.31 MM-MG
252. C
5.9 HPS
4.817 30-M
49815. SCMH
103171. ACMM
105.9
.0000
.0000 MG/OSCM
.000 KG/HR
U>
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 02-2
OUTLET STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO * (17.647 • VM * Y • (PB * PM / 13.6)) / (TM * 460.)
17.647 • 59.865 * 1.004 * ( 29.51 * .797 / 13.6)
VMSTO » ————— ——————— — . = 62.678 OSCF
( 40. » 460.)
VOLUME OF NATER VAPOR AT STANDARD CONDITIONS
VNC * .04707 • VLC
VNC * .04707 • 182. * 8.56 SCF
PERCENT MOISTURE IN STACK GAS
BNO » (100. • VNC) / (VMSTD » VNC)
^. 100. • 8.56
7 BNO « — ——— ...... c 12.02 PERCENT
U) 62.678 » 8.56
MOLE FRACTION OF DRY STACK GAS
FMO * (100. > BNO) / 100.
100. . 12.0
FMO • ————— ——— « .880
100.
AVERAGE MOLECULAR NEIGHT OF DRY STACK GAS
MD * (PC02 * .44) » (P02 * .32) * (PN2 * PCO) * .28
MO * ( 4.30*44/100) «• (12.3*32/100) » ((83.4+ .0) * 28/100 = 29.18
MOLECULAR NEIGHT OF STACK GAS
MNS * MO * (1. > (BNO/100)) * 18. * (BNO/100)
MNS * 29.18* (1. •(12.02/100)) * 18. * (12.02/100) * 27.84
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP * SUM. OF THE SORT(VH * (TS » 460.))
VS « 85.49 * CP • OELP / (SQRT(MNS • PS) * PNTS)
VS « 85.49 * .64 • 93.346 / (SORM 87.84 * 39.42) * 12. » 19.52 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS « 19.52 « 1466. 3600/144 s 3643425. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO « 17.647 * OS * P3 • (1. • (BNO/100)) / (TS * 460.)
17.647 * 3645425. * 29.42 • (1. • (12.02/100))
OSSTO * —— • — » 1759182. 3CFH
( 486. » 460.)
>
I PERCENT I30KINETIC
u>
£ ISO • (305.58*(T3+460.))«((0.002669«VLC)+(VM*Y*(P8+(PM/13.6))/(TM»460.)))/(TT«VS*PS«DN*DN)
(305.58M 486.+460.))*((0.002669* 182.)+( 59.865*1.004*( 29.51+( .797/13.6))/( 40.+460.)))
j30 . ..... .. .... ... . . ... . s 105.85 PERCENT
120. * 19.52 * 29.42 * .400 * .400
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS » 0.001 • MN • 15.43 / VMSTO
CS « 0.001 * .0000 * 15.43 / 62.678 s .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR • CS * OSSTD / (15.43 * 453.6)
PMR * .00000 * 1759182. / (15.43 * 453.6) * .00000
-------
Run No. D2.2
3
Sample volume = 1.78m r 62.68 scf
Example calculations
CS (Part) =38.3/1.78 =21.5 mg/m3
CS (Part) = 0.001 x38.3 x 15.43/62.68 =0.009 qr/dscf
CS (S02) = 159.4*1.78= 89.6 ma/m3
= 89.6 x 24.067 64 =34 pom
= 0.001 x159.4x 15.43/_6Z^8_ = 0.039 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
38.3
24.6
2.6
3.5
2.0
159.4
14.4*
N/A
N/A
N/A
3 Concentration,
mg/m
21.5
13.8
1.5
2.0
1.1
89.6
8.1
gr/dscf
0.009
0.006
0.001
0.001
0.001
0.039
0.004
ppm
34
2
*Field analysis.
A-343
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(OEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND OHIO
STACK OUTLET *t BATTERY
PART/H2S04/S02
DAN FITZGERALD
20.
29. 51
-1.20
3530341
97.75 .00
.81
133
.000 CFM a 6.5 IN.HG
.982
DATE
NUN NUMBER
PMOBE LENGTH ft TYPE
NUZZLE : 1.0.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
PETER BOX NUMBER
METER HEAD OIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
K FACTOR
12/iu/ai
02-3
4 FOOT GLASS
.404
13.7
FB6
1.91
350.
350.
12337.4
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE CLOCK
TIME TIME
(MIN.) (20-HR
CLOCK)
GAS METER VELOCITY ORIFICE PRESSURE STACK
READING HEAD DIFFERENTIAL TEPP
(CU.FT.) (IN.H20) (IN.H20) (DEG.F)
DESIRED ACTUAL
DRY GAS METER PUMP SAMPLE
TEMP VACUUM BOX TEMP
(DEG.F) (IN.HG) (UEG.F)
IMPINGER
TEMP
(DEG.F)
INLET OUTLET
1NIT
co
TOTALS
AVERAGE
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
120.0
1310
1320
1330
1340
1350
1400
1410
1420
1430
1440
1450
1500
1510
695.528
700.300
705.335
710.200
714.650
720.000
725.200
729.600
734.600
740.100
744.200
749.600
754.460
58.932
.060
,067
.068
.061
.065
.064
.066
.068
,060
.064
.063
.062
.77
.88
.88
.60
.84
.85
.84
.89
.79
.84
.82
.80
.83
.77
.88
.88
.80
.84
.85
.84
.89
.79
.84
.82
.80
.83
500.
481.
489.
478.
491.
465.
505.
476.
491.
474.
488.
496.
486.
36.
41.
44.
45.
45.
45.
45.
45.
45.
45.
45.
45.
44.
35,
35.
35.
35.
35.
35.
35.
35.
35.
35,
35.
35.
35.
2.5
.0
.0
.0
.0
.0
.0
.0
.0
.0
.5
.5
360.
363.
361.
366.
370.
373.
361.
334.
377.
367.
363.
365.
4.8 363.
37.
39.
40.
40.
37.
40.
40.
54.
60.
55.
55.
55.
46.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST D2-3
STACK OUTLET HI BATTERY
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1
to VM
(ji ...
TM
VMSTD
VLC
VMC
BMO
FMO
PC02
P02
PCO
PN2
MD
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR MT-ORY STACK GAS
MOLECULAR XT-STACK GAS
ENGLISH UNITS
12/10/61
1310
1510
120.0
12
.962
.404 IN
.84
.83 IN-H20
58.932 CU-FT
39.4 F
60.470 SCF
180.6
8.501 SCF
12.33
.677
4.30
12.30
.00
83.40
29.18
27.80
METRIC UNITS
12/10/61
1310
1510
120.0
12
.982
10.3
.84
21.2
1.669
4.1
1.712
180.6
.241
12.33
.877
4.30
12.30
.00
83.40
29.18
27.60
MM
PM-H20
CU-M
c
SCK
SCK
-------
PB
PSI
PS
TS
VS
AS
OSSTD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES Of STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOM RATE, DRY*
ACTUAL STACK FLO* RATE
PERCENT ISOKINETIC
MG. EPA 5
84.51 IM-HG
-1.20 IN-H20
29.42 IN-HG
466. F
19.5 FPS
T505. SO-IN
1763133. SCFH
3664702. ACFH
100.4
.0000
.00000 GR/DSCF*
.00000 LB/HR
EMISSION RATE
* 66 DEC F, 29.92 IN.HG.
749.55 KM-HG
•30.48 PM-H20
747.31 KM-HG
252. C
6.0 I* PS
4.842 SQ-M
49927. SCKH
103773. ACPH
100.4
.0000
.0000 MG/DSCM
.000 KG/HR
U)
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 02-3
STACK OUTLET *1 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VM9TD « (17.647 * VM * Y * (PB * PM / 13.6)) / (TM «• 460.)
17.647 • 56.932 * .962 • ( 29.51 + .633 / 13.6)
VMSTD » .......-....— — — .-——- —............ . i 60.470 OSCF
I 39. * ObO.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC « .04707 • VLC
VHC • .04707 * 161. = 6.50 SCF
PERCENT MOISTURE IN STACK GAS
BWO • (100. * VMC) / (VMSTD * VHC)
100. * 8.50
SMO « ——. ... * 12.33 PERCENT
60.470 * 6.50
MOLE FRACTION OF DRY STACK GAS
FMD * (100. > BNO) I 100.
100. * 12.3
FMD s —— ..... ..... * .877
100.
AVERAGE MOLECULAR WEIGHT OF DRV STACK GAS
MD • (PC02 * .44) * (P02 * .32) » (PN2 * PCD) • .26
MD * ( 4.30*44/100) «• (12.3*32/100) * ((83.4* .0) * 26/100 = 29.18
MOLECULAR HEIGHT OF STACK GAS
MHS s MD * (1. > (BHO/100)) » 18. * (BHO/100)
MN3 * 29.18* (1. '(12.33/100)) » 18. * (12.33/100) s 27.60
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SQRMVH * (TS + 460.))
VS • 85.49 * CP • DELP / (SORT(MnS * PS) * PNTS)
VS « 85.49 • .84 • 93.354 / (SORT ( 27.80 * 29.43) * \Z. = 19.53 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS * VS • AS • 3600/144
OS » 14.53 * 7505. 3600/144 a 3664702. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO « 17.647 • OS • PS * (1. - (BWO/100)) / (TS * 460.)
17.647 • 3664702. * 29.42 * (1. - (12.33/100))
OS8TD • • —— = 1763133. SCFH
( 486. * 460.)
>
^ PERCENT ISOKINETIC
GO ISO * (305.58*(TS»460.))*((0.002669*VLC)*(VM*Y*(PB»(PH/13.6))/(TM»460.)))/(TT*VS*PS*DN*ON)
(305.58*( 486.+460.))*((0.002669* 181.)*( 58.932* .982*( 29.51t( .833/13.6))/( 39.+460.)))
ISO * ———————-——.—- ————-—-- — -- ——..................................—....... s 100.40 PERCENT
120. * 19.53 * 29.42 * .404 • .404
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
CS » 0.001 * .0000 * 15.43 / 60.470 = .00000 GR/DSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR « CS * QSSTD / (15.43 * 453.6)
PMR s .00000 * 1763133. / (15.43 * 453.6) = .00000
-------
Run No.02.3
o
Sample volume = 1.71 m .60.47 scf
Example calculations
CS (Part) =34.8 /I.71 . 20.4 mq/m3
CS (Part) = 0.001 x 34.8 x 15.43/60.47 = 0.009 qr/dscf
CS (S02) =155.0/1.71 = 90.6 ma/m3
= 90.6 x 24.06/64 = 34 ppm
= 0.001 xl55.0 x 15.43/60.47 = Q.Q4Q gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H2S04
As H2S04.2H20
Water soluble sulfates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
34.8
0.6
0.8
3.5
155.0
8.7
N/A
N/A
N/A
3 Concentration,
mg/m
20.4
0.3
0.5
2.0
90.6
5.1
gr/dscf
0.009
0.0001
0.0001
0.001
0.040
0.002
ppm
34
1
A-349
-------
FIELD DATA
I
CO
Ul
o
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET #1
SAMPLE TYPE PART/HeSD4/SU2
OPERATOR DAN FITZGERALD
AMBIENT TEMP.(OEG.F) 20.
BAR. PRESS. (IN.HG) 29.51
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530311
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .84
THERM. NO. 133
LEAKAGE .000 CFM a 6.
METER CALIB. FACTOR 1.033
READ & RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
1312
1322
1332
1342
1352
1402
1412
1422
1432
1442
1452
1502
1512
EVERY 10.0
GAS METkR
READING
(CU.FT.)
253.209
257.945
262.940
268.415
273.160
277.600
282.600
287.500
293.800
297.800
302.900
307.600
312.205
MINUTES
VELOCITY
HEAD
(IN.H20)
.060
.067
.068
.061
.065
.064
.066
.068
.060
.064
.063
.062
CLEVELAND OHIO
BATTERY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.77
.88
.88
.80
.84
.85
.84
.89
.79
.84
.82
.80
H20)
ACTUAL
.77
.88
.88
.80
.84
.85
.84
.89
.79
.84
.82
.80
STACK
TEPP
(DEG.F)
500.
481.
489.
478.
491.
465.
505.
476.
491.
474.
488.
496.
DATE 12/10/A1
HUN NUMBER 02-4
PROBE LENGTH 8 TYPE 4 FOOT GLASS
NOZZLE : I.D. .404
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
PETEK BOX NUMBER FB4
PETEN HEAD DIFF. 1.88
PROBE HEATER SETTING 350.
HEATER BUX SETTING 350.
K FACTOR 12337.4
DRY GAS METER
TEMP
(OEG.F)
INLET OUTLET
40. 40.
42. 40.
45. 38.
46. 39.
47. 39.
48. 39.
48. 39.
48. 39.
48. 39.
48. 39.
48. 39.
48. 39.
PUMP
VACUUM
(IN.HG)
2.5
3.0
3.0
3.0
4.5
4.5
4.5
5.0
5.0
5.0
5.0
5.5
SAMPLE
BOX TEMP
(DEG.F)
400.
405.
389.
395.
387.
388.
373.
373.
396.
381.
370.
385.
IMPINGER
TEMP
(DEG.F)
42.
40.
39.
40.
41.
40.
56.
54.
64.
60.
60.
60.
TOTALS
AVERAGE
120.0
58.996
.83
.83 486.
46.
39.
4.2 387.
50.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST D2-4
STACK OUTLET HI BATTERY
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
U) UM
Ul
TM
VMSTO
VLC
VNC
BNO
FMD
PC02
P02
PCO
PN2
MO
MNS
TIME-START
TIME-FINISM
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPUR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
12/10/81
1312
1512
120.0
12
1.033
.404 IN
.84
.83 IN-H20
58.996 CU-FT
42.7 F
63.263 SCF
184.6
8.689 SCF
12.08
.879
4.30
12.30
.00
83.40
29.18
27.83
METRIC UNITS
12/10/81
1312
1512
120.0
12
1.033
10.3
.84
at. a
1.671
5.9
1.791
184.6
.246
12.08
.879
4.30
12.30
.00
83.40
29.18
27.83
I'M
MM-H20
CU-M
C
SCK
3CM
-------
PB
P3I
PS
T3
VS
AS
Q33TO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
3TACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE, DRY*
ACTUAL STACK FLOW RATE
PERCENT 1SOK1NETIC
MG. EPA 5
EMISSION RATE
* 6B DEG F, 29.« IN.HG.
29.51 1N-HG
•1.20 1N-H20
29.43 IN-HG
086. r
19.5 FPS
7505. 30-IN
1767255. SCFH
3662869. ACFH
104.B
.0000
.00000 GR/OSCF*
.00000 LB/HR
7Q9.55 HM-HG
-30.06 MM-M20
747.31 KM-HG
252. C
6.0 fPS
0.812 30-M
50003. SCMH
103721. ACMM
104.B
.0000
.0000 MG/D3CM
.000 KG/HR
co
01
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 02-4
STACK OUTLET «1 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 • VM • 1 • (P8 * PM / 13. 6)) / (TM + 460.)
17.647 • 58.996 * 1.033 • ( 29.51 + .833 / 13.6)
VMSTD • — — — --- - --------------- - ------------------------ = 63.263 OSCF
( 43. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC e .04707 * VLC
VNC « .04707 • 185. * 8.69 SCF
PERCENT MOISTURE IN STACK GAS
BMO « (100. • VMC) / (VMSTO * VWC)
100. * 8.69
BMO « — — — --- ..... ---------- - s 12.08 PERCENT
jp 63.263 * 8.69
I
l_r.-
Ul
W MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BMO) / 100.
100. - 12.1
FMD * ————————— * .879
100.
AVERAGE MOLECULAR MEIGHT OF DRY STACK GAS
MD • (PC02 * .44) * (P02 * .32) * (PN2 » PCO) * .28
MD = ( 4.30*44/100) » (12.3*32/100) * ((83. 4* .0) * 26/100 = 29.18
MOLECULAR MEIGHT OF STACK GAS
MHS a MO * (1. - (BNO/100)) * 18. * (BNU/100)
MMS * 29.18* (1. -(12.08/100)) * 18. * (12.08/100) s 27.63
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SURHVH * (TS «• 460.))
VS « 85.49 * CP • DELP / (SORT(MWS * PS) * PNTS)
VS « 85.49 * .84 * 93.354 / (SORT( 27.83 * 29.42) * 12. = 19.52 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
US * VS * AS • 3600/144
QS » 19.52 * 7505. 3600/144 a 3662869. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTD * 17.647 * OS * PS * (1. • (BMO/100)) / (TS » 460.)
17.647 * 3662869. * 29.42 * (1. • (12.08/100))
OSSTO « — ——— a 1767255. SCFH
( 486. * 460.)
,p PERCENT ISOKINETIC
U> ISO » (305.5B*(TS+460.))*((».002669«VLC)»(VM*Y*(PB»(PM/13.6))/(TM*460.)))/(TT*V8«PS*DN*DN)
(Ji
^ (305.5B*( 486.*460.))*((0.002669* 185.)*( 58.996*1.033*( 29.51*( .833/13.6))/( 43.«460.)))
ISO « ————————————————[[[ 3 104.79 PERCENT
120. * 19.52 • 29.42 * .404 * .4V4
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS • 0.001 * MN • 15.43 / VM3TD
CS « 0.001 * .0000 * 15.43 / 63.263 > .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMH * CS * QSSTD / (15.43 * 453.6)
-------
Run No. D2.4
Sample volume = 1.79 m T 63.26 scf
Example calculations
CS (Part) =37.2/1.79 = 20.8 mg/m3
CS (Part) = 0.001 x 37.2 x 15.43/63.26 = 0.009 qr/dscf
CS (S02) =131.8/1.79 =73.6 mg/m3
= 73.6 x 24.06/64 = 28 pom
= 0.001 x 131.8x 15.43/62x2fi_BOa2. gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H2S04
As H2S04-2H20
Water soluble sulfates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
37.2
0.4
0.5
4.8
131.8
54.8
N/A
N/A
N/A
3 Concentration,
mg/m
20.8
0.2
0.3
2.7
73.6
30.6
gr/dscf
0.009
0.0001
0.0001
0.001
0.032
0.013
ppm
28
8
A-355
-------
FltlO DATA
U)
01
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE STACK
SAMPLE TYPE M5-250
OPERATOR DU
AMBIENT TEMP. (DEG.F) 28.
BAR. PRESS. (IN. HG) 29.51
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBERtS) 3530003
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .83
THERM. NO.
LEAKAGE .000 CFM 0 3.
METER CAL1B. FACTOR .992
READ ft RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
PI nr * \
IIUCK I
1310
1320
1330
1340
1350
1400
1410
1420
1430
1440
1450
IbUO
1510
EVERY 10.0
GAS METER
READING
(CU.FT.)
925.417
931.070
936.220
941.400
946.600
951.860
957.100
962.320
967.550
972.810
978.100
983.320
988.572
MINUTES
VELOCITY
HEAD
(IN.H20)
.060
.060
.060
.060
.060
.060
.060
.060
.060
.060
.060
.060
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
STACK
DIFFERENTIAL TE^P
(IN.
DESIRED
.89
.89
.89
.89
.89
.09
.89
.89
.89
.89
.89
.89
H20)
ACTUAL
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
(OEG.F)
501.
481.
489.
478.
491.
505.
465.
477.
491.
474.
488.
496.
OATE 12/10/81
RUN NUMBER D2-5
PROBE LENGTH S TYPE 6* GLASS
N02ZLE : 1.0. .431
ASSUMED MOISTURE 13.7
SAMPLE BUX NUMBER
ME1EH BOX NUMBER FBI
METER HEAD DIFF. i.«7
C FACTOR .71
PROBE HEATER SETTING 250.
HEATER BUX SETTING 250.
REFERENCE PRESS. DIFF. .12
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
43. 36.
43. 35.
46. 36.
49. 36.
52. 37.
54. 3».
55. 39.
55. 39.
55. 39.
55. 40.
55. 40.
55. 40.
PUMP
VACUUM
(1N.H8)
2.0
2.0
2.0
2.1
2.2
2.2
2.2
2.2
2.2
2.2
2.2
2.2
SAMPLE
BOX TEMP
(DEG.F)
268.
253.
193.
258.
318.
268.
268.
247.
291.
249.
218.
270.
IMPINGER
TEMP
(DEG.F)
3«.
34.
33.
35.
35.
35.
34.
34.
38.
38.
37.
37.
TOTALS
AVERAGE
120.0
63.155
.89
.89 486.
51.
38.
2.1
258.
35.
-------
PARTICIPATE FIELD DATA a RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DU
TEST D2-5
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
1 VM
OJ
cn
~J TM
VMSTD
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
ENGLISH UNITS
12/10/81
1310
1510
120. 0
12
.992
.431 IN
.63
.69 IN-H20
63.155 CU-FT
44.7 F
64.791 SCF
METRIC UNITS
12/10/81
1310
1510
120.0
12
.992
10.9
.83
22.6
1.788
7.0
1.835
CM
KM-M20
CU-M
C
SCK
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VMC VOLUME OF WATER VAPOR
AT STANDARD CONDITIONS*
BWO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.* DRY
P02 PERCENT 02 BY VOL.. DRV
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL.. DHY
MD MOLECULAR hT-ORY STACK GAS
MMS MOLECULAR WT-STACK GAS
190.7
8.976 SCF
190.7
.251 SCI*
12.17
.878
4.30
12.30
.00
63.40
29.18
27.82
12.17
.878
4.30
12.30
.00
83.40
29.18
27.82
-------
Pb
PSI
PS
TS
vs
AS
OSSTO
OS
ISO
MN
cs
PHR
BAROMETRIC PKESSUHE
STATIC PRES OF STACK GAS
STACK PRESr ABS.
AVERAGE STACK TEMP
AV6 STACK 6AS VELOCITY
STACK AREA
STACK FLO* HATE* DHt*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
29.51 IN-HG
•1.20 IN-H20
29.02 IN-HG
066. F
18.7 FPS
7066. SO-1N
1680969. SCFH
3488292.
98.6
.0000
ACFH
.00000 GR/DSCF*
.00000 LB/HR
709.55 CM-HG
•50.08 I»l»i-H20
707.31 KM-HG
252. C
5.7 CPS
0.817 SO-M
07bOO. SCCH
98778. ACI»H
98.6
.0000
.0000 MG/DSCH
.000 KG/Hfi
EMISSION RATE
* 68 DEG Ft 29.92 IN.HG.
U)
Ul
00
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NU. 02-5
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD = (17.607 • VM * Y * (PB » PM / 13.6)) / (TM » 060.)
17.647 • 63.155 • .99? * ( 39.51 » .890 / 13.6)
VMSTD = ——.——. — — — — — — — ———.. — .. — . — s 60.791 DSCF
I 05. * 060.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC = .00707 * VLC
VHC = .00707 • 191. s 8.98 SCF
PERCENT MOISTURE IN STACK GAS
BNO = (100. * VHC) / (VMSTD » VHC)
•p 100. « 8.98
I 8HO = --— — — — --- - ------- --- = 12.17 PERCENT
U) 60.791 » 8.V8
ID
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - 8*0) / 100.
100. - 12.3
FMD = — — — — — ---- — ---- = .878
100.
AVERAGE MOLECULAR HEIGHT OF DRV STACK GAS
HD = (PC02 * .00) * (P02 * .32) * (PN2 * PCO) • .28
MD = ( 0.30*00/100) «• (12.3*32/100) » ((83. 0* .0) * 28/100 = 29.18
MOLECULAR HEIGHT OF STACK GAS
MHS = MD * (1. - (BWU/10U)) + 18. * (8X0/100)
MWS = 29.18* (1. -(12.17/100)) * 18. * (12.17/100) = 27.82
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THt SURT(VH • ITS + 060.))
VS = 85.49 * CP * DELP / (SOHT(MNS * PS) • PNTS)
VS = 85.49 • .83 • 90.421 / ISQHT( 27.88 * 29.42) • lef. = IB.69 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS = VS * AS * 3600/144
OS = 10.69 * 7466. 3600/144 = 348B292. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD = 17.647 * OS * PS * (1. - (BNU/100)) / (TS * 460.)
17.647 * 3488292. * 29.42 * (1. - (12.17/100))
OSSTD = -—------— ...... .... = 1600969. SCFH
( 486. + 460.)
>
I PERCENT ISOKINETIC
Lo
O 130 = (305.58*(TS+46U.))«((0.002669*VLC)»(VM*Y*(PB»(PM/13.6))/(TM»460.)))/(TT*V3*PS*DN*ON)
1305.58*( 486.+460.))*((0.002669* 191.)*( 63.155* ,992*( 29.51+1 .890/13.6))/( 45.«460.)))
130 a ——. —-— — — ................. .................................... ...... • 98.63 PERCENT
120. * 18.69 * 29.42 * .431 * .431
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 • MN * 15.43 / VMSTD
CS = 0.001 * .0000 * 15.43 / 64.791 = .00000 GR/OSCF
PAHTICULATE LBS/HR -- tPA METHOD 5
PMR = CS * OSSTO / (15.43 • 453.6)
PMR = .00000 * 1680969. / (15.43 * 453.6) = .00000
-------
Run No. D2-5
Sample volume =1.84 m3t64.79 scf
Example calculations
CS (Part) =41.1 /1.84= 22.3 rnq/m3
CS (Part) = 0.001 x 41.1 x 15.43^4.79 =0.010 qr/dscf
CS (S02) = /.
mg/nf
= x 24.OS/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
41.1
23.4
19.2
18.8
17.7
15.1
0.0
0.0
0.0
N/A
N/A
152.6
0.8
8.6
3 Concentration,
mg/m
22.3
12.7
10.4
10.2
9.6
8.2
0.0
0.0
0.0
82.9
0.43
4.7
gr/dscf
0.010
0.005
0.004
0.004
0.004
0.003 .
0.000
0.000
0.000
0.036
0.0002
0.002
ppm
A-361
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(OEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBEH(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
COKE STACK
M8-660
00
28.
39.51
-1.20
3530202
97. 50 .00
.83
CFM a 10.0 IN.HG
DATE 12/10/81
RUN NUPBER 02-6
PROBE LENGTH ft TYPE 5" GLASS
NOZZLE : I.D. .378
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
ff.1f.tt BOX NUMBER FBb
fETEH hEAO DIFF. 1.51
C FACTOR .90
PROBE HEATER SETTING 600.
HEATER BOX SETTING 600.
REFERENCE PRESS. DIFF. .17
.967
READ ft RECORD DATA EVERY 10.0 MINUTES
I
U)
LUI. n t
1311
1321
1331
13
-------
PARTICULATE FIELD DATA R RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO
TEST D2-6
COKE STACK
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
W VM
OJ
TM
VMSTD
VLC
VMC
BHO
FMD
PC02
P02
PCO
PN2
MD
MHS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPUH
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 HY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR HT-ORY STACK GAS
MOLECULAR KT-STACK GAS
12/10/81
1311
1511
120.
12
.
.
.
•
58.
35.
59.
168.
7.
11.
.
4.
12.
.
83.
29.
27.
0
967
378 IN
83
63 IN-H20
333 CU-FT
8 F
317 SCF
3
922 SCF
78
882
30
30
00
no
18
86
METRIC UNITS
12/10/81
1311
1511
120.0
12
.967
9.6
.83
16.0
1.6b2
2.1
1.681
168.3
.224
11.78
.882
a. 30
12.30
.00
83. 00
29.18
27.86
PP
MM-H20
CU-M
C
SO
SCf
-------
PB
PS1
PS
TS
VS
AS
QSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE, DRY*
ACTUAL STACK F|_0» HATE
PERCENT ISOKINETIC
MG. EPA 5
>
cr\
EMISSION RATE
* 68 DEC F, 89.1)2 IN.HG.
29.51 IN-HG
-1.20 IN-H2U
29.12 IN-HG
4Bb. F
18.7 FPS
7466. SQ-IN
1687140. SCFH
3185548. ACFH
117.0
.0000
.00000 GR/DSCF*
.00000 LB/HR
749.55 fM-HG
-30.48 KH-H20
747.31 PM-HG
252. C
5.7 KPS
4.017 SQ-M
47775. SC^H
98700. ACKH
117.0
.0000
.0000 MG/DSCM
.000 KG/HR
-------
EXAMPLE PAHTICULATE CALCULATIONS TEST NO. D2-6
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD a (17.647 * VM * y * (PB * PM / 13.6)) / (TM » 460.)
17.647 • 56.333 * .967 * ( 29.51 * .630 / 13.6)
VMSTD » ————...- —.... — .———.-..................- = 59.307 DSCF
( 36. + 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC = .04707 * VLC
VMC = .04707 * 168. r 7.92 SCF
PERCENT MOISTURE IN STACK GAS
BMO * (100. * VMC) / (VMSTD + VMC)
to 100. • 7.92
I BMO = — — —— ..._.— r 11.78 PERCENT
LO 59.347 + 7.92
Ul
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - BMO) / 100.
100. - 11.8
FMD = ————— ——--- s .882
100.
AVERAGE MOLECULAR MEIGHT OF DRY STACK GAS
MD * (PC02 * .44) * (P02 * .32) » (PN2 * PCO) • .28
MO s ( 4.30*44/100) » (12.3*32/100) » ((83.a* .0) * 28/100 * 29.18
MOLECULAR MEIGHT OF STACK GAS
MMS s MD * (1. - (BMO/100)) «• 18. * (8*0/100)
MMS = 29.16* (t. -(11.76/100)) * 18. * (11.76/100) = 27.86
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SClrtMVH * ITS * . + 4bO.)
>
U) PERCENT ISOKINETIC
CT>
171 ISO = (305.58*(TS*4bO.))* ( (0.002669*VLC) + (VM*Y*(PB*(PM/13.6))/(TM»460.)))/(TT*VS«PS*DN*ON)
(305.58M 486.»460.))*((0.002669* 168.)+( 58.333* ,967*( 29.51»( .630/13.6))/( 36.»460.)))
ISO s ................ . ....... .. ............ ..................................... » 117.03 PERCENT
120. * 18.67 * 29.42 * .378 * .378
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 * MN * lb.43 / VMSTD
CS = 0.001 * .0000 * 15.43 / 59.347 = .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR s CS * OSSTD / (15.43 » «53.6)
PM« s .00000 * 1687140. / (15.43 * 453.6) s .00000
-------
Run No. D2.6
Sample volume =1.68 m r 59.35 scf
Example calculations
CS (Part) =30.3/1.68 = 18.0 mg/m3
CS (Part) = 0.001 x30.3 x 15.43/59.35= 0.008 qr/dscf
CS (S02) = 152.8/1.68 = 91.0 ma/m3
= 91.0 x 24.06^4 = 34ppm
= 0.001 x!52.8x 15.43£a*35__ = JLlMDgr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
30.3
<0.3
<0.4
<0.3
152.8
10.7
o Concentration,
mg/m
18.0
<0.2
<0.3
<0.2
91.0
6.4
gr/dscf
0.008
0.0001
0.0001
0.0001
0.040
0.003
ppm
34
2
A-367
-------
FIELD DATA
UJ
c^
00
PLANT REPUBLIC STEEL
SAMPLING LOCATION OUTLET STACK
SAMPLE TYPE PART/H2S04/S02
OPERATOR CB
AMBIENT TEMP.(OEG.F) 26.
BAR. PRESS. (IN. HG) 29.55
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530025
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .63
THERM. NO.
LEAKAGE .002 CFM S H.
METER CALIB. FACTOR 1.003
READ * RECORD DATA
TRAVERSE
POINT
NO.
1N1T
SAMPLE
TIME
(MIN.)
0
4.0
10.0
20.0
30.0
40.0
50.0
60.0
fo. o
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
r i rif* M \
ULUIK 9
1131
1141
1350
1400
1410
1420
1430
1440
1450
1500
1510
1520
1530
1540
EVERY 10.0
GAS METER
READING
(CU.FT.)
361.265
362.966
366.660
371.160
375.330
379.750
383.570
387.200
391.130
395.030
398.880
402.560
407.170
411.081
MINUTES
VELOCITY
HEAD
(IN.H20)
.055
.046
.049
.046
.050
.038
.035
.042
.000
.040
.043
.044
.045
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.72
.62
.64
.62
.65
.50
.46
.54
.52
.52
.56
.57
.58
H20)
ACTUAL
.72
.62
.64
.62
.65
.50
.46
.54
.52
.52
.56
.57
.5S
STACK
TECP
(DEG.F)
475.
496.
506.
470.
460.
485.
482.
500.
466.
480.
4B5.
505.
485.
DATE 12/11/81
NUN NUMBER 03-1
PWOBE LENGTH A TYPE 5* HEATEO GLASS
NOZZLE : 1.0. .401
ASSUMED KOISTUHE 14.0
SAMPLE BOX NUVBER 0
fETEH BOX NUMBER FB2
METE* HEAD DIFF. 1.76
C FACTUK .82
HRUet hfcATEk SETTING 250.
HEATER BOX SETTING 250.
KEFEHENCE PHESS. DIFF. .14
DRY GAS PblER
TECP
(DEG.F)
INLET OUTLET
35. 33.
35. 32.
35. 32.
36. 32.
40. 32.
44. 34.
46. 36.
48. 36.
48. 36.
48. 37.
48. 3B.
48. 38.
48. 30.
PUMP
VACUUM
(IN.Hb)
2.0
2.0
2.0
3.0
2.0
2.0
2.0
2.0
2.U
3.0
3.u
3.0
3.0
SAMPLE
BOX TEfP
(UEG.F)
275.
247.
269.
246.
24^.
252.
240.
250.
247.
250.
239.
230.
230.
IKP1NGEK
TEMP
(OEG.F)
0.
35.
37.
42.
46.
44.
51.
50.
4".
50.
52.
54.
54.
TOTALS
AVERAGE
120.0
49.816
.58
.58
486.
43.
35.
2.4
248,
43.
-------
PAHTICULATE MELO 1>ATA * RESULTS TABULATION
PLANT* NAME ANU AOORkSS ttST TEAM LEAUtH
REPUBLIC STtEL CLEVELAND CB
TtST
1)5-1
OUTLM STACK
TtST DATE
TB TIME-START
TF TIME-FINISH ...
TT NET TIME OF TEST, MIN.
NP NET SAMPLING POINTS
Y METER CALIBRATION FACTOR
ON SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMH
VMSTO VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL M20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VNC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMD MULE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR HT-DRY STACK GAS
MNS MOLECULAR NT-STACK GAS
ENULISM UNITS
1131
Ht IK 1C UNI TS
1131
120.0
13
1.003
.401 IN
.83
.58 IN-H20
49.816 CU-FT
39.0 F
52.294 SCF
122.4
5.761 SCF
9.92
.901
4.00
12.00
.00
84.00
29.12
2B.02
180.0
13
1.003
10.2
.83
14.7
1.411
3.9
1.461
122.4
.163
9.92
.901
4.00
12.00
.00
84.00
29.12
28.02
MM
MM-H20
CU-M
c
sec
SCt"
-------
PB
P3I
PS
TS
VS
AS
QSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE, DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
EMISSION RATE
* 68 DEC f, 29.92 IN.HG.
29.55 IN-HG
-1.20 IN-H20
29.46 IN-HG
086. F
16.0 FPS
7466. SO-IN
1476086. SCFH
2981939. ACFH
104.7
.0000
.00000 GR/DSCF*
.00000 LB/HR
750.57 KM-HG
-30.48 KM-H20
748.33 fM-HG
252. C
4.9 UPS
4.817 SO-M
41798.
84440.
104.7
.0000
.0000 MG/OSCM
.000 KG/HR
UJ
•J
O
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. D3-1
OUTLET STACK
VOLUME OF D»Y GAS SAMPLED AT STANDARD CONDITIONS
VM8TD * (17.647 • VM • Y * (PB * PM / 13.6)) / (TM + 460.)
17.647 * 49.816 • 1.003 * ( 29.55 «• .577 / 13.6)
VMSTD » — — ----- — *— — . ------------- ....... ---------- a 52.294 03CF
t J9. » a*o.)
VOLUME OP MATER VAPOR AT STANDARD CONDITIONS
VMC « .04707 * VLC
VMC » .04707 * 122. « 5.76 3CF
PERCENT MOISTURE IN STACK GAS
BNO « (100. * VMC) / (VMSTD + VMC)
"f 100. • 5.76
U) BMO = ————————— s 9.92 PERCENT
52.294 * 5.76
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - BMO) / 100.
100. - 9.9
FMD = — — ————— — — = .901
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MD s (PC02 • .44) * (P02 * .32) * (PN2 * PCO) * .28
MO • ( 4.00*44/100) * (12.0*32/100) + ((61.0+ .0) * 26/100 = 29.12
MOLECULAR MEIGHT OF STACK GAS
MHS = MD « (1. - (BHO/100)) * 18. * (BhO/100)
MMS s 29.12* (1. •( 9.92/100)) » 18. * ( 9.92/100) = 28.02
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP * SUM. OF THE SORT(VH * (TS * 160.))
VS • 85.49 • CP * DELP / (SORMMKS * PS) * PNTS)
VS * 85.49 * .83 * 84.090 / (SORT( 38.08 • 89.06) * 13. = 15.98 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS « VS * A3 * 3600/144
OS * 15.98 * 7466. 3600/144 = 2981939. ACFH
STACK GAS VOLUMETRIC FLOH AT STANDARD CONDITIONS
OSSTD • 17.647 • 03 * PS • (1. • (6*0/100)) / (TS * 460.)
17.647 * 2981939. * 29.46 »(!.-( 9.92/100))
OSSTD = ----———.-.— — - — --— .......... .. = 1476086. SCFH
( 486. * 460.)
PERCENT ISOKINETIC
ISO = (305.58*(T3*460.))*((0.002669*VLC)*(V»'*Y*(PB*{PM/13.6))/(TM«.460.)))/(TT*V3*PS*DN*ON)
(305.5B*( 486.+460.))*((0.002669* 122.)+( 49.816*1.003*( 29.55#( .577/13.6))/( 39.4060.)))
ISO » = 104.73 PERCENT
120. * 15.98 * 29.46 * .401 * .401
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
CS * 0.001 * .0000 * 15.43 / 52.294 = .00000 6R/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR r CS * OSSTD / (15.43 * 453.6)
PMR c .00000 * 1476086. / (15.43 • 453.6) = .00000
-------
Run No. D3.1
Sample volume - 1.48 m3r 52.29 scf
Example calculations
CS (Part) = 38.6/1.48 = 26.1 mq/m3
CS (Part) = 0.001 x 33.6 x 15.43/52.29 = 0.011 qr/dscf
CS (S02) = 90.I/ 1.48= 60.9 ma/m3
= 60.9 x 24.06/64 = 23 ppm
= 0.001 x 90.1 x 15.43/52.29 = 0.026 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
38.6
0.3
0.4
6.0
90.1
84.0
3 Concentration,
mg/m
26.1
0.2
0.3
4.0
60.9
56.8
gr/dscf
0.011
0.0001
0.0001
0.002
0.026
0.025
ppm
23
14
A-373
-------
FIELD OAT*
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
OUTLET STACK
PART/H2S04/SU2
BHUFFEY
28.
29.55
-1.20
3530309
97.50 .00
.83
.003 CFM 9
1.024
5.0 IN.HG
READ & RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE CLOCK
TIME TIME
(MIN.) (24-HR
CLOCK)
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H2U)
ORIFICE PRESSURE STACK
DIFFERENTIAL TEMP
(IN.H20) (DEG.F)
DATE 12/01/81
RUN NUMBER D3-2
PROBE LENGTH ft TYPE 4* GLASS
NOZZLE t I.D. .401
ASSUMED MOISTURE 14.0
SAMPLE BOX NUMBER g
PETER BOX NUMBER FB7
METER HEAD OIFF. .71
C FACTOR .84
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. OIFF. .14
DRY GAS METER PUMP SAMPLE
TEMP VACUUM BOX TEMP
(DEG.F) (IN.HG) (DEG.F)
IMPINGER
TEMP
(DEG.F)
DESIRED ACTUAL
INLET OUTLET
1NIT
>
-J
0
r.o
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
40.0
100.0
110.0
120.0
1134
1141
1350
1400
1410
1420
1430
1440
1450
1500
1510
1520
1530
1540
TOTALS
AVERAGE
120.0
483.135
486.635
489.200
493.770
496.350
502.950
507.640
511.800
515.680
519.900
524.000
528.470
532.990
537.320
54.185
.055
.048
.048
.048
.050
.038
.035
.042
.040
,040
.043
.044
,045
.72
.62
.62
.62
.65
.50
.46
.54
.52
.52
.56
.57
.58
.58
.72
.62
.62
.62
.65
.50
.46
.54
.52
.52
.56
.57
.58
475.
498.
508.
470.
480.
485.
482.
500.
505.
466.
480.
485.
485.
.58 486.
40.
40,
44,
48.
50.
52.
55.
56.
56.
56.
56.
56,
56.
51,
36.
36.
36.
36.
38.
40.
42.
42.
44.
45.
45.
45.
46.
41.
2.0
2.5
2.5
2.5
3.0
3.0
3.0
3.0
3.5
4.0
4.2
4.2
4.2
310
295
300
272
276
260
265
262
253
258
250
245
245
3.2 270.
0.
39.
44.
44.
47.
47.
55.
53.
55.
55.
55.
54.
54.
46.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND BRUFFEY
TEST D3-2
OUTLET STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
1
OJ VM
TM
VMSTO
VLC
VNC
BHO
FMD
PC02
P03
PCQ
PN2
MD
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BY VOL., DRV
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR WT-ORV STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
12/01/81
1134
1540
120.0
13
1.024
.401 IN
.83
.58 IN-H20
54.185 CU-FT
46.2 F
57.246 SCF
144.7
6.811 SCF
10.63
.894
4.00
12.00 .
.00
84.00
29.12
27.94
METRIC UNITS
12/01
1134
1540
120.0
13
1.024
10.2
.83
14.6
1.534
7.9
1.621
144.7
.193
10.63
.894
4.00
12.00
.00
84.00
29.12
27.94
/81
I'M
PM-H20
CU-M
C
sec
SCP
-------
PB
PSI
PS
TS
VS
AS
OSSTO
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK G»S
STACK PRES, ABS.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE* DRY*
ACTUAL STACK FLON RATE
PERCENT ISOKINETIC
MG. EPA S
29.55 IN-HG
-1.20 1N-H20
29.06 IN-MG
086. F
16.0 FPS
7066. SO-IN
1065237. SCFH
29B3501. ACFH
115.5
.0000
.00000 GR/DSCF*
.00000 LB/HR
750.57 KM-HG
•30.08 MM-H20
708.33 CM-HG
252. C
0.9 KPS
0.817 SQ-M
01091.
81080.
115.5
.0000
.0000 MG/DSCM
.000 KG/HR
EMISSION RATE
* 68 OEG F, 29.92 IN.H6.
CJ
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. D3-2
OUTLET STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.607 • VM * Y * (PB » PM / 13.6)) / (TM * 060.)
17.607 • 50.185 • 1.020 * ( 29.55 * .575 / 13.6)
VMSTD s ...................... ......... ........... - 57.206 DSCF
( 06. + 060.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC = .00707 * VLC
VMC * .00707 * 145. = 6.81 9CF
PERCENT MOISTURE IN STACK GAS
BMO « (100. * VMC) / (VMSTD * VMC)
100. * 6.81
BMO « — — = 10.63 PERCENT
57.246 + 6.81
MOLE FRACTION OF DRY STACK GAS
FMO = (100. - BMO) / 100.
100. > 10.6
FMD * ———————— s .890
100.
AVERAGE MOLECULAR WEIGHT OF DRV STACK GAS
MD s (PC02 * .44) » (P02 * .32) * (PN2 * PCO) * .28
MD a ( 4.00*44/100) * (12.0*32/100) » ((80.0* .0) * 28/100 s 29.12
MOLECULAR WEIGHT OF STACK GAS
MMS « MD * (1. - (BHO/100)) * 18. * (BftO/100)
MMS = 29.12* 11. -(10.63/100)) » 18. * (10.63/100) * 27.90
-------
STACK GAS VELOCITY »T STACK CONDITIONS
DELP = SUM. OF THE SQRT(VH * (TS «• 460.))
VS « 85.49 * CP * DELP / (SORT(MWS * PS) * PNTS)
VS * 85.49 * .83 * 84.016 / (SQRT( 27.94 * 29.46) * 13. = 15.98 FPS
STACK 6AS VOLUMETRIC FLON AT STACK CONDITIONS
OS » VS « AS • 3600/144
OS = 15.98 * 7466. 3600/144 » 2983501. ACFH
STACK CAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD * 17.647 * OS * PS * (I. - (8WO/100)) / (TS * 460.)
17.647 * 2983501. * 29.46 • (1. - (10.63/100))
OSSTD s .........................—........................ s 1465237. SCFH
( 486. «• 460.)
> PERCENT ISOKINETIC
^ ISO * (305.58*(TS+460.))*((0.002669*VLC)+(VM*Y*(PB+(PI*/13.6))/(TM4460.)))/(TT*VS*PS*DN*DN)
00
(305.5BM 486.»460.))*((0.002669* 145.)*( 54.185*1.024* ( 29.55*( .575/13.6))/( 46.+ 460.)))
ISO * . . — = 115.49 PERCENT
120. * 15.98 * 29.46 * .401 * .401
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTO
CS « 0.001 * .0000 * 15.43 / 57.246 = .00000 GR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR = CS * OSSTD / (15.43 * 453.6)
PMR z .00000 * 1465237. / (15.43 * 453.6) s .00000
-------
Run No. D3.2
Sample volume =1.62 m , 57.25 scf
Example calculations
CS (Part) =34.5/1.62 = 21.3 mq/m3
CS (Part) = 0.001 x34.5 x 15.43,57.25 = 0.009 qr/dscf
CS (S02) =152.Ei/1.62= 94.3ma/m3
= 94.3 x 24.06/64 =35 ppm
= 0.001 x!52.8x 15.43/57.25 = Q.Q41 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
34.5
18.1
1.8
2.5
0.0
152.8
7.0
o Concentration,
mg/m
21.3
11.2
1.1
1.5
0.0
94.3
4.3
gr/dscf
0.009
0.005
0.0005
0.001
0.000
0.041
0.002
ppm
35
1
A-379
-------
FIELD DATA
UJ
00
o
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET *1
SAMPLE TYPE PART/H2S04/S02
OPERATOR DAN FTIZGERALl)
AMBIENT TEMP. (DEG.F) 26.
BAR. PRESS. (IN.HG) 29.55
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530345
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .84
THERM. NO. 133
LEAKAGE .004 CFM 3 10.
METER CALIB. FACTOR .962
HEAD & RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
pi nr v ^
LLUCn )
1134
1353
1403
1413
1423
1433
1446
1453
1503
1513
1523
1533
1542
GAS METER
READING
(CU.FT.)
754.742
759.100
763.255
767.550
771.675
775.930
779.750
783.375
787.225
791.165
794.960
798.960
803.032
VELOCITY
HEAD
(IN.H20)
.055
.046
.054
.048
.050
.038
.035
.042
.040
.040
.043
.044
CLEVELAND OHIO
BATTERY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
OFSIREO
.68
.58
.65
.60
.62
.47
.03
.51
.48
.50
.53
.54
H20)
ACTUAL
.68
.58
.65
.60
.62
.47
.43
.51
.48
.50
.53
.54
STACK
TEMP
(DEG.F)
DATE 12/11/81
RUM NUMBER 03-3
PHOBE LENGTH ft TYPE 4 FOOT GLASS
NOZZLE : I.D. .402
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
MFTER BOX NUMBER FB8
METER HEAD OIFF. 1.91
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
K FACTOR 11628.0
DRY GAS METER
TEMP
(DEG.F
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPINGEH
TEMP
(DEG.F)
INLFT OUTLET
175.
496.
506.
470.
480.
485.
4«2.
500.
505.
466.
480.
485.
39.
35.
38.
42.
45.
47.
48.
50.
51.
52.
53.
54.
38.
33.
33.
34.
35.
36.
38.
40.
41.
42.
43.
44.
9.0
8.0
9.0
4.0
10.0
8. 5
7.5
7.5
7.5
7.5
8.0
6.0
369.
442.
406.
411.
411.
414.
430.
409.
398.
410.
407.
399.
40.
44.
48.
47.
50.
52.
55.
55.
59.
57.
60.
60.
TOTALS
AVERAGE
120.0
46.290
.55
.55
486,
46,
38,
8.3 411.
52.
-------
PARTICIPATE FIELD DATA « RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FTIZGERALO
TEST 03-3
STACK OUTLET 01 BATTERY
U)
DO
TEST DATE
TB TIME-START
TF TIME-FINISH
TT NET TIME OF TEST, M1N.
NP NET SAMPLING POINTS
Y METER CALIBRATION FACTOR
ON SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL HZO COLLECTED IN
IMPINGERS AND SILICA GEL,»L.
VNC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BHO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRV GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL.* DRV
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR MT-DRY STACK GAS
MNS MOLECULAR NT-STACK GAS
ENGLISH UNITS
12/11/81
1130
1542
120.0
12
.982
.002 IN
.84
.55 IN-H20
48.290 CU-FT
42.1 F
49.315 SCF
143.2
6.740 SCF
12.02
.880
4.00
12.00
.00
84.00
29.12
2T.78
METRIC UNITS
12/11/81
1134
1542
120.0
12
.982
10.2
.84
13.9
1.367
5.6
1.396
143.2
.191
12.02
.880
4.00
12.00
.00
84.00
29.12
27.78
KM
CM-H20
CU-M
C
SCf
sec
-------
PB
PSI
PS
TS
VS
AS
OSSTO
OS
ISO
HN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, A8S.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE, DRY*
ACTUAL STACK FLOM RATE
PERCENT ISOKINETIC
MG. EPA 5
EMISSION RATE
68 DEC F, 29.92 IN.HG.
89.55 IN-HG
•1.20 IN-H20
29.46 IN-HG
486. F
16.3 FPS
7505. 30-IN
1077970. SCFH
3057331. ACFH
96.7
.0000
.00000 GR/OSCF*
.00000 LB/HR
750.57 KM-HG
•30.40 HM-H20
748.33 *M-MG
252. C
5.0 fPS
4.842 SQ-M
11852. SCHH
86574. *CfH
98.7
.0000
.0000 MG/OSCM
.000 KG/MR
U)
00
to
-------
"~co
U)
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 03-3
STACK OUTLET »l BATTERY
VOLUME OF ORT GAS SAMPLED AT STANDARD CONDITIONS
VMSTO « (17.647 • VM • Y • (PB * PM / 13.6)) / (TM * 460.)
17.647 • 48.290 • .982 * ( 29.55 * .549 / 13.6)
VMSTD f - ---------------------------------------------------- = 49.315 DSCF
( 42. + 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC * .04707 • VLC
VMC s .04707 * 143. = 6.74 SCF
PERCENT MOISTURE IN STACK GAS
BMO « (100. « VMC) / (VMSTD » VHC)
100. * 6.74
• ---------------- — * 12.02 PERCENT
49.315 * 6.74
MOLE FRACTION OF DRY STACK GAS
FMD « (100. • BMO) / 100.
100. - 13. 0
FMD * .—.——————— z .880
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO « (PC02 * .44) * (POZ * .32) * (PN2 * PCO) * .28
MD = ( 4.00*44/100) » (12.0*32/100) * ((BO.O+ .0) * 28/100 = 29.12
MOLECULAR HEIGHT OF STACK GAS
MHS > MO * (1. - (BHO/100)) + 18. * (BHO/100)
M*S * 29.12* (I. •(12.02/100)) » 18. * (12.02/100) a 27.78
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP » SUM. OF THE SORT(VH * (TS » 060.))
VS * 85.39 * CP * DELP / (SORT(Ml»S * PS) * PNTS)
VS « 85.49 • .84 * 77.908 / (SORT( 27.78 * 29.46) • 12. = 16.30 FPS
STACK GAS VOLUMETRIC FLOM AT STACK CONDITIONS
OS a vs * AS * 3600/100
OS * 16.30 * 7505. 3600/100 « 3057331. ACFH
STACK GAS VOLUMETRIC FLOH AT STANDARD CONDITIONS
OSSTD « 17.647 * OS * PS * fl. - (BNO/100)) / (TS * 460.)
17.647 * 3057331. • 29.46 * (1. • (12.02/100))
OSSTO a = 1077970. SCFH
( 486. «• 460.)
> PERCENT ISOKINETIC
I
jj£ ISO * (305.5B*(T3*460.))*((0.002669*VLC)*(VM*Y*(PB»(PM/13.6))/(TM»460.)))/(TT*VS«P3*DN*OM
*>
(305.5B*( 486.+460,))*((0.002669* 143.)*( 48.290* ,982«( 29.55»( .549/13.6))/( 42.4460.)))
130 * ......-.....-..................................._................................................ z 98.65 PERCENT
120. * 16.30 * 29.06 • .402 • .402
PARTICIPATE LOADING -- EPA METHOD 5 (AT STANDARD CONDITIONS)
CS » 0.001 * MN * 15.43 / VMSTO
CS = 0.001 * .0000 * 15.43 / 49.315 = .00000 GH/OSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR s CS * OSSTD / (15.43 * 453.6)
PMR s .00000 • 1477970. / (15.43 * 453.6) * .00000
-------
Run No. D3.3
Sample volume = 1.40m3T 49.32scf
Example calculations
CS (Part) =30.9/1.40 = 22.1 mq/m3
CS (Part) = 0.001 x30.9 x 15.43/19.32 = 0.010 qr/dscf
CS (S02) = 130.8/1.40 = 93.4ma/m3
= 93.4 x 24.06/64 = 35 pom
= 0.001 x130.8x 15.4349.32 = Q.Q41 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
30.9
0.0
0.0
4.1
130.8
12.0
3 Concentration,
mg/m
22.1
0.0
0.0
2.9
93.4
8.6
gr/dscf
0.010
0.000
0.000
0.001
0.041
0.004
ppm
35
2
A-385
-------
FIELD DATA
GJ
00
PLANT REPUBLIC STEtL
SAMPLING LOCATION STACK OUTLET «1
SAMPLE TYPE PART/H2S04/S02
OPERATOR DAN FTIZGERALO
AMBIENT TEMP.(OEG.F) 28.
BAR. PRESS. (IN. HG) 29.55
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530513
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. ,8a
THERM. NO. 133
LEAKAGE .014 CFM 3 5.
METER CALIB. FACTOR 1.033
READ * RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
00.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
PI nr it i
LLULK )
1139
1358
1408
1418
1428
1438
144(1
1458
1508
1518
1528
1538
1548
EVERY 10.0
GAS METER
READING
(CU.FT.)
312.428
316.815
320.830
325.155
329.265
333.490
337.130
340.640
344.525
348.100
351.965
356.310
360.313
MINUTES
VELOCITY
HEAD
(IN.H20)
.055
.048
.054
.048
.050
.038
.035
.042
.000
.040
.043
.044
CLEVELAND OHIO
BATTERY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.68
.58
.65
.60
.62
.47
.43
.51
.48
.50
.53
.54
H20)
ACTUAL
.68
.58
.65
.60
.62
.47
.43
.51
.48
.50
.53
.54
STACK
TEMP
(DEG.F)
475.
498.
508.
470.
400.
485.
482.
500.
505.
466.
480.
485.
DATE 12/11/81
RUN NUMBER D3-4
PROBE LENGTH ft TYPE 5 FOOT GLASS
NOZZLE : I.U. .401
ASSUMED MOISTURE 13.2
SAMPLE BOX NUMBER
METER BOX NUMBER FB4
METER HEAD OIFF. i.ss
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
K FACTOR 11628.0
DRY GAS METER PUMP
TEMP VACUUM
(DEG.F) (IN.HG)
INLET OUTLET
43. 42.
39. 33.
42. 38.
47. 39.
49. 40.
51. 42.
53. 43.
53. 44.
54. 45.
55. 47.
57. 48.
59. 50.
.0
.0
.5
.0
.0
.0
.0
.5
.0
.5
.5
.5
SAMPLE
BOX TEMP
(OEG.F)
404.
440.
400.
404.
392.
409.
422.
415.
395.
395.
360.
364.
IMPINGER
TEMP
(DEG.F)
42.
46.
50.
50.
53.
56.
60.
59.
60.
59.
61.
59.
TOTALS
AVERAGE
120.0
47.885
.55
.55
480,
50.
43.
3.6 400.
55.
-------
PARTICIPATE FIELD DATA s RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO OAN FTIZGERALO
TEST D3-4
STACK OUTLET »1 BATTERY
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
OJ VM
CXI
TM
VMSTD
VLC
VNC
BHO
FMO
PC02
P02
PCO
PN2
MD
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,HL.
VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR MT-DRY STACK GAS
MOLECULAR HT-STACK GAS
ENGLISH UNITS
12/11/81
1139
1548
120.0
12
1.033
.001 IN
.64
.55 IN-H20
47.885 CU-FT
46.4 F
51.009 SCF
141.1
6.642 SCF
11.52
.885
4.00
12.00
.00
84.00
29.12
27. BO
METRIC UNITS
12/11/81
1139
1548
120.0
12
1.033
10.2
.84
13.9
1.356
8.0
1.004
141.1
.188
11.52
.885
4.00
12.00
.00
84.00
29.12
27.84
MM
MM-H20
CU-M
C
SCM
SCM
-------
PB
PSI
PS
TS
VS
AS
OSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE, DRV*
ACTUAL STACK FLO* RATE
PERCENT ISOKINETIC
MG. EPA 5
29.55 IN-HG
•1.20 IN-H20
?9.06 IN-HG
«BO. F
lb.2 FPS
7505. SO-IN
1«89756. SCFH
3002559. ACFH
101.7
.0000
.00000 GR/DSCF*
.00000 LB/HR
750.57 PM-HG
•30.ae VM-H20
708.33 HM-MG
C
a.9 fPS
a.602 SO-M
SCMH
B6156. »CMH
101.7
.0000
.0000 MG/DSCM
.000 KG/HR
EMISSION RATE
• 68 DE6 F, 29.92 IN.HG.
OJ
00
00
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 03-0
STACK OUTLET «l BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD a (17.647 • VM • Y • (PB * PM / 13.6)) / (TM •» 860.)
17.647 * 47.885 • 1.033 • ( 29.55 * ,50<> / 13.6)
VMSTD a —— — —— —-.. — - — = 51.009 OSCF
C 46. + 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC 3 .04707 * VLC
VNC * .04707 * 141. a 6.64 3CF
PERCENT MOISTURE IN STACK GAS
BMO • (100. * VMC) / (VMSTO * VMC)
100. * 6.64
BMO * = 11.5? PERCENT
> 51.009 + 6.64
CO
00
ID
MOLE FRACTION OF DRY STACK GAS
FMO = (100. - BMO) / 100.
100. - 11.5
FMO a — —— . — a .885
100.
AVERAGE MOLECULAR MEIGHT OF DRY STACK GAS
MD a (PC02 • .44) * (P02 * .32) «• (PN2 * PCO) • .28
MO = ( 4.00*44/100) * (12.0*32/100) * ((84.0* .0) * 28/100 = 29.12
MOLECULAR HEIGHT OF STACK GAS
MMS a MD * (1. • (BHO/100)) » 18. * (BWO/100)
MMS = 29.12* (1. -(11.52/100)) * 18. * (11.52/100) = 27.84
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SQRT(VH • (TS * 460.))
VS = BS.49 * CP * DELP / (SURT(MHS * PS) * PNT3)
VS = 85.49 * .84 * 77.610 / (SQRT( 87.80 * 89.46) * 18. = 16.22 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS * VS • AS * 3600/144
OS a 16.22 * 7505. 3600/144 « 3042559. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD * 17.64? * OS * PS * (1. - (BWO/100)) / (TS * 460.)
17.647 * 3042559. * 29.46 * (1. - (11.52/100))
OSSTD * — = 1489756. SCFH
( 4«0. *• 460.)
PERCENT I30KINETIC
>
jjj ISO ~ (305.5e*(TS*460.))*((0.002669*VLC)»(VK*Y*(PB'»(P*/13.6))/(TM»460.)))/(TT*VS*PS*DN*DN)
VD
O (305.58*( 480.4460.))*((0.002669* 141.)*( 47.885*1.033* ( 29.59*( .549/13.6))/( «6.«460.)))
ISO » ..... . . * 101.74 PERCENT
120. * 16.22 * 29.46 * .401 * .401
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 • MN * 15.43 / VMSTO
CS * 0.001 * .0000 * 15.43 / 51.009 = .00000 GR/DSCF
PARTICIPATE LBS/HR -- EPA METHOD 5
PMR » CS * OSSTD / (15.43 * 453.6)
PMR a .00000 * 1489756. / (15.43 * 453.6) c .00000
-------
Run No. D3.4
Sample volume = 1.44m3T 51.01 scf
Example calculations
CS (Part) =38.7/1.44=26.9 mg/m3
CS (Part) = 0.001 x38.7 x 15.43/51.01 = 0.012 qr/dscf
CS (S02) =143.4/1.44 =99.6 ma/m3
= 99.6 x 24.06/64 =37 ppm
= 0.001 x143.4 x 15.43/51.01 = 0.043 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
38.7
1.9
2.6
0.8
143.4
8.2
3 Concentration,
mg/m
26.9
1.3
1.8
0.5
99.6
5.7
gr/dscf
0.012
0.001
0.001
0.0002
0.043
0.002
ppm
37
1
A-391
-------
FIELD DATA
>
U)
PLANT REPUBLIC SUEL
SAMPLING LOCATION CUKE STACK
SAMPLE TYPE M5-250
OPERATOR 00
AMBIENT TEMP. (OEG.F) 28.
BAR. PRESS. (IN. HG) 29.55
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 5530110
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .83
THERM. NO.
LEAKAGE .000 CFM a) 3.
METER CALIB. FACTOR .99?
READ • RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
00.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
n nr* i
tL.Ul.~J
1145
1354
1404
1414
1424
1434
1444
1454
1504
1514
1524
1534
1544
EVERY 10.0
GAS METER
READING
(CU.FT.)
988.766
993. B70
998.960
4.060
9.180
14.330
19.490
24.680
29.880
35.090
40.300
45.510
50.756
MINUTES
VELOCITY
HEAD
(IN.H2U)
.056
.056
.056
.056
.056
.056
.056
.056
.056
.056
.056
.056
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.86
.86
.86
.86
.86
.86
.86
.86
.86
.86
.86
.86
H20)
ACTUAL
.86
.86
.86
.86
.86
.86
.86
.86
.86
.86
.86
.86
STACK
TEMP
(OEG.F)
«75.
498.
508.
470.
480.
485.
482.
500.
505.
466.
480.
485.
DATE 12/11/81
RUN NUKBER 03-5
PROBE LENGTH ft TYPE 5* GLASS
NOZZLE : I.U. .434
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
METEH BOX NUMBER FBI
PETER HEAD OIFF. 1.87
C FACTOR .71
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .12
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
«3. 37.
42. 36.
45. 36.
51. 37.
56. 39.
60. 42.
61. 43.
62. 45.
64. 47.
65. 47.
65. 48.
64. 48.
PUMP
VACUUM
(IN.HG)
.5
.5
.5
.0
.0
.0
.0
.0
.0
.0
.0
.5
SAMPLE
BOX TEMP
(DEG.F)
228.
297.
243.
279.
236.
254.
282.
232.
280.
231.
219.
268.
IMPINGEK
TEMP
(OEG.F)
38.
38.
38.
39.
40.
40.
38.
38.
42.
44.
45.
46.
TOTALS
AVERAGE
120.0
61.990
.86
.86
486.
57.
42.
.9 254.
41.
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND 00
TEST D3-5
COKE STACK
TEST DATE
TB
If
TT
NP
Y
DN
CP
PM
I VM
OJ
vo
W TM
VMSTD
VLC
VWC
8*0
FMO
PC02
P02
PCO
PN2
MO
HNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRV GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR KT-STACK GAS
ENGLISH UNITS
12/11/81
lias
isofl
120.0
12
.992
.030 IN
.83
.86 IN-H20
61.990 CU-FT
49.3 F
63.099 SCF
101.1
6.602 SCF
9.52
.905
0.00
12.00
.00
80.00
29.12
2«.06
METRIC UNITS
12/11
1105
1500
120.0
12
.992
11.0
.83
21.8
1.755
9.6
1.787
101.1
.186
9.52
.905
4.00
12.00
.00
84.00
29.12
28.06
/81
I'M
KM-H20
CU-M
C
sec
SCM
-------
PB
PSI
PS
TS
VS
AS
(JSSTD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE. DRY*
ACTUAL STACK FLO* RATE
PERCENT ISOKINETIC
M6. EPA 5
EMISSION RATE
* 68 OE6 F, 29.92 IN.HG.
29.55 IN-HG
•I.SO IN-H20
29.06 IN-HG
OH6. F
10.0 FPS
7066. Sn-IN
1666931. SCFH
3352B85. ACFH
95.5
.0000
.00000 GR/OSCF*
.00000 LB/HR
750.57 MM-HG
-30.48 CM-H20
708.33 *M-HG
252. C
5.5 *P3
4.817 SQ-M
17202. 3Cm
90944. »CCH
95.5
.0000
.0000 MG/DSCM
.000 KG/MR
>
co
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. D3-5
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD e (17.647 * VM • Y * (PB » PM / 13.6)) / (TM * 460.)
17.647 • 61.990 • .993 • ( 39.55 » .860 / 13.6)
VMSTO s ———————. .......... ....... . . 63.099 DSCF
( 49. + 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC s .04707 * VLC
VHC 3 .04707 * 141. 3 6.64 SCF
PERCENT MOISTURE IN STACK GAS
BHO 3 (100. • VHC) / (VMSTO * VHC)
100. • 6.64
BHO 3 — ...... - 9.52 PERCENT
63.099 + 6.64
MOLE FRACTION OF DRY STACK GAS
FMD 3 (100. - BHO) / 100.
100. - 9.5
FMD 3 — ....... . = .905
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD 3 (PC02 * .44) » (P02 * .33) * (PN3 «• PCO) • .28
MD 3 ( 4.00*44/100) » (13.0*32/100) + ((84.0* .0) * 36/100 s 39.12
MOLECULAR HEIGHT OF STACK GAS
MHS 3 MO * (1. - (BHO/100)) * 18. * (BWO/lOO)
MHS 3 39.12* (1. -( 9.52/100)) * 18. * ( 9.52/100) s 38.06
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SORTtVH • (TS » 060.))
VS * 85.49 * CP • OELP / (SORMMKS * PS) * PNTS)
VS = 85.19 * .83 * 87.347 / (SOHT( 88.06 « 29.46) * 12. = 17.96 FP3
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS = VS • AS • 3600/144
03 * 17.96 • 7466. 3600/144 * 3352885. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO = 17.647 • OS » PS • (1. - (BWO/100)) / (TS * 460.)
17.647 « 3352885. * 29.46 •(!.-( 9.52/100))
OSSTO * —..————— — - —.. . .. a 1666931. SCFH
( 486. » 460.)
PERCENT ISOKINETIC
t>
I ISO * (305.58*(TS*460.))*((0.002669*VLC)*(VM*Y*(PB'MPM/13.6})/(TM»460.)))/(TT*VS*P3*DN*DN)
U)
J£ (305.58*1 486.+460.))*((0.002669* 141.)*( 61.990* .992*( 29.55+t .860/1J.6))/( O9.«460.)))
ISO s • — — = 95.53 PERCENT
1?0. * 17.96 • 29.46 * .434 * .034
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 * MN * 15.43 / VMSTD
CS * 0.001 * .0000 * 15.43 / 63.099 = .00000 GR/DSCF
PARTICULATE LB3/HR — EPA METHOD 5
PMR = CS * 03STD / (15.43 * 453.6)
PMR s .00000 * 1666931. / (15.43 * 453.6) = .00000
-------
Run No. D3.5
Sample volume = 1.79 m3. 63.10 scf
Example calculations
CS (Part) = 35.0/1.79 =19.6 mq/m3
CS (Part) = 0.001 x 35.0 x 15.43/63.10 =0.008 qr/dscf
CS (S02). = / = mg/m3
= x 24.06/ = ppm
= 0.001 x,
.x 15.43/.
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
35.0
22.2
19.9
15.7
15.7
13.4
0.0
0.0
0.9
28.9
2.0
3.4
3 Concentration,
mg/m
19.6
12.4
11.1
8.8
8.8
7.5
0.0
0.0
0.5
16.1
1.1
1.9
gr/dscf
0.008
0.005
0.005
0.004
0.004
0.003
0.000
0.000
0.0002
0.007
0.0005
0.0008
ppm
A-397
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBERO)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALI8. FACTOR
REPUBLIC STEEL
COKE STACK
M8-600
00
28.
29.55
-1.20
3530218
97.50 .00
.63
CLEVELAND
.016 CFM 9
.967
10.5 IN.HG
READ & RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
CLOCK)
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE STACK
DIFFERENTIAL TEPP
(IN.H20) (OEG.F)
DATE 12/11/81
RUN NUPBER 03-6
PROBE LENGTH ft TYPE 4* GLASS
NOZZLE : I.D. .379
ASSUMED MOISTURE 13.7
SAPPLE BOX NUPBER
PETER BOX NUPBEN FB6
PETER HEAD OIFF. 1.51
C FACTUR .90
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .16
DRY GAS METER PUMP SAPPLE
TEMP VACUUM BOX TEMP
(DEG.F) (IN.HG) (DEG.F)
IPPINGEH
TEMP
(OEG.F)
DESIRED ACTUAL
INLET OUTLET
1N1T
co
vo
oo
TOTALS
AVERAGE
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
120.0
1137
1356
1406
1416
1426
1436
1446
1456
1506
1516
1526
1536
1546
741.956
746.950
751.960
756.990
762.060
767.060
772.060
777.130
782.200
787.270
792.340
797.420
802.493
60.537
.056
.056
.056
.056
.056
.056
.056
.056
.056
.056
.056
.056
.63
.63
.63
.63
.63
,63
.63
,63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
.63
«75.
498.
508.
470.
480.
485.
482.
500.
505.
466.
480.
485.
.63 486.
35.
34.
37.
43.
48.
51.
52.
52.
53.
53.
53.
52.
47,
35.
35.
35.
35.
36.
38.
39.
40.
42.
42.
42.
42.
38.
3.3
3.4
3.6
3.7
3.7
4.0
4.8
6.2
7.4
8.0
8.7
9.2
517
555
546
536
534
547
538
538
538
538
522
524
5.5 536.
42.
41.
40.
40.
40.
40.
42.
42.
44.
44.
46.
46.
42.
-------
PARTICULATE FIELD DATA « RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND 00
TEST D3-6
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
> PM
^° VM
vo
TM
VMSTD
VLC
VNC
BViO
FMD
PC02
P02
PCO
PN2
MO
MNS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZ7LE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR MT-STACK GAS
ENGLISH UNITS
12/11/81
1137
1506
120.0
12
.967
.379 IN
.83
.63 IN-H20
60.537 CU-FT
02.7 F
60.820 SCF
160.5
7.703 SCF
11.29
.887
0.00
12.00
.00
HO. 00
29.12
27.86
METRIC UNITS
12/11/81
1137
1546
120.0
12
.967
9.6
.83
16.0
1.710
5.9
1.722
164.5
.219
11.29
.887
4.00
12.00
.00
84.00
29.12
27.86
fM
KM-H20
CU-M
C
SCM
SCM
-------
PB
PSI
PS
T3
VS
AS
OSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEHP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE, DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
39.55 IN-HG
-1.20 IN-H20
29.46 IN-HG
486. F
18.0 FPS
7466. Sn-IN
1640093. SCFH
3364702. ACFH
122.7
.0000
.00000 GR/OSCF*
.00000 LB/HR
750.57 *M-HG
•30.48 PM-H20
748.33 fM-HG
252. C
5.5 WPS
4.817 SO-M
46443. SCKH
95278. ACMH
122.7
.0000
.0000 MG/OSCH
.000 KG/HR
EMISSION RATE
* 68 DEG F, 29.92 IN.HG.
O
O
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. os-6
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 * VM * Y * (P8 «• PM / 13.6)) / (TM * 460.)
17.647 • 60.537 * .967 • ( 39.55 * .630 / 13.6)
VM3TD = —— — . = 60.824 DSCF
I 43. «• 4bO.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC * .04707 * VLC
VKC f .04707 « 165. = 7.74 SCF
PERCENT MOISTURE IN STACK GAS
BMO * (100. * VMC) / (VMSTD * VMC)
> 100. • 7.74
' BMO « —————— ......—. = 11.29 PERCENT
O 60.824 » 7.74
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - BHO) / 100.
100. • 11.3
FHD s —.——.—............ 3 .887
100.
AVERAGE MOLECULAR WEIGHT OF DRV STACK GAS
MO = (PC02 • .44) + (P02 * .32) * (PN2 «• PCO) • .28
MD = ( 4.00*44/100) » (12.0*32/100) + ((80.0* .0) * 28/100 = 29.12
MOLECULAR HEIGHT OF STACK GAS
MHS = MD • (1. - (BVO/100)) + 18. * (BWQ/100)
MMS e 29.12* (1. -(11.29/100)) * IB. * (11.29/100) « 27.86
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SHRT(VH * (TS » 060.))
VS s 85.
^ PERCENT I30KINETIC
o
M ISO * (305.58*(TS+060.))*((».002669*VLC)+(VMoYo(PB»(PM/13.6))/(TM4060.)))/(TT*VS*PS*DN*ON)
(305.58M 086.+060.))*((0.002669* 165.)+( 60.537* .967*( 29.55*( .630/13.6))/( O3.»060.)))
ISO « . — s 122.73 PERCENT
120. * 18.03 * 29.06 • .379 * .379
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS < 0.001 * MN * 15.03 / VMSTD
CS = 0.001 * .0000 * 15.03 / 60.820 = .00000 GR/DSCF
PAHTICULATE LBS/HR — EPA METHOD 5
PMR = CS * OSSTD / (15.03 * 053.6)
PMR = .00000 * 1600093. / (15.03 * 053.6) s .00000
-------
Run No. D3.6
Sample volume =1.72 m3. 60.82 scf
Example calculations
CS (Part) =25.5/1.72=0.006 mg/m3
CS (Part) = 0.001 x25.5 x 15.43/60.82=0.006 qr/dscf
CS (S02) =169.VI.72= 98.3ma/m3
= 98.3 x 24.06^4 =37 ppm
= 0.001 x 169.1 x 15.43/_&L£2_ = QJM3_ gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H2S04
As H2S04-2H20
Water soluble sulfates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
25.5
0.0
0.0
2.2
169.1
12.8
o Concentration,
mg/m
14.8
0.0
0.0
1.3
98.3
7.4
gr/dscf
0.006
0.000
0.000
0.0005
0.043
0.003
ppm
37
2
A-403
-------
FIELD DATA
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OOTLET 01
SAMPLE TYPE PAHT/H2S04/S02
OPERATOR ARMSTRONG
AMBIENT TEMP.(OEG.FJ 35.
BAH. PRESS. (IN. H6) 39.72
STATIC PRESS. (IN. H2U) -1.20
FILTER NUMBERtS) 3530325
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .80
THERM. NO. 133
LEAKAGE .000 CFM 9 7.
METER CALIB. FACTOR 1.003
READ » RECORD DATA
TRAVERSE
POINT
NO.
1NIT
SAMPLE
TIME
(MIN.)
V
10.0
20.0
30.0
00.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HH
PI up w i
ILUIK 1
940
950
1000
1010
1020
1030
1040
1050
1100
1110
1120
1130
1140
EVERY 10.0
GAS METER
READING
(CU.FT.)
411.613
416.200
420.910
425.660
430.260
435.130
439.830
444.630
449.380
454.000
458.800
463.800
468.564
MINUTES
VELOCITY
HEAD
(IN.H20)
.047
.U50
.048
.050
.053
.049
.052
.048
.050
.051
.056
.050
CLEVELAND OHIO
BATTERY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.62
.66
.64
.66
.70
.65
.68
.64
.66
.67
.74
.66
H20)
ACTUAL
.62
.66
.64
.66
.70
.65
.68
.64
.66
.67
.74
.66
STACK
TEfP
(DEG.F)
487.
495.
507.
474.
485.
498.
483.
499.
510.
474.
482.
490.
DATE 12/12/81
HUN NUMBER ua-i
PROBE LENGTH t TYPE 5 FOOT GLASS
NOZZLE : I.D. .404
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
KE1ER box NUMBErt FB2
METER HEAD D1FF. 1.7b
C FACTOh .80
PROBE HEATER SETTING 250.
HEATER BUX SETTING 250.
REFERENCE PRESS. OIFF. .14
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
38. 37.
40. 37.
42. 37.
44. 38.
45. 38.
46. 38.
46. 38.
46. 38.
47. 40.
48. 40.
48. 40.
48. 4U.
PUfP
VACUUM
(IN.HG)
2.5
3.0
3.0
3.5
5.0
5.0
5.0
5.0
5.5
6.0
6.5
7.0
SAMPLE
BOX TEMP
(OEG.F)
292.
304.
320.
304.
315.
302.
319.
315.
301.
285.
266.
266.
IMPIN6ER
TEMP
(DEG.F)
37.
37.
44.
45.
«7.
«6.
50.
50.
53.
52.
53.
55.
TOTALS
AVERAGE
120.0
56.951
.67
.67
490.
45.
38.
4.8 299,
47.
-------
PARTICULATE FIELD DATA « RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LtADEH
REPUBLIC STEEL CLEVELAND OHIO ARMSTRONG
TEST D4-1
STACK OUTLET ft| BATTERY
TEST DATE
TB
TF
TT
NP
Y
ON
CP
I PM
O
V VM
TM
VMSTD
VLC
VWC
BNO
FMD
PC02
P02
PCO
PN2
MD
MftS
TIME-START
TIME-FINISH
NET TIMt OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 bY VOL., DRY
MOLECULAR |»T-OKY STACK GAS
MOLECULAR WT-STACK GAS
ENGLISH UNITS
12/12/81
940
1140
120.0
12
1.003
.404 IN
.84
.67 IN-H20
56.951 CU-FT
41.6 F
59.821 SCF
157.3
7.404 SCF
11.01
,B<)0
3.70
11.10
.00
85.20
29.04
27.62
METRIC UNITS
12/12/81
940
1140
120.0
12
1.003
10.3
.84
16.9
1.613
5.3
1.694
157.3
.210
11.01
.890
3.70
11.10
.00
85.20
29.04
27.82
KM
fM-H20
CU-M
C
SCK
SCM
-------
PB
PSI
PS
TS
VS
AS
QSSTO
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, A6S.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE* DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
I
£>
O
EMISSION RATE
* 68 DEG F, 29.92 IN.HG.
29.72 IN-HG
-1.20 IN-H20
29.63 IN-HG
490. F
17.3 FPS
7505. SO-IN
1586494. SCFH
3244223. ACFH
1 10.2
.0000
.00000 GR/DSCF*
.00000 LB/HR
754.89 KM-HG
-30.48 KM-H20
752.65 CM-HG
255. C
5.3 CPS
4.842 SO-M
44981. SCKH
91867. ACCH
110.2
.0000
.0000 HG/OSCM
.000 KG/HR
-------
EXAMPLE PART1CULATE CALCULATIONS TEST NO. DO-1
STACK OUTLET «1 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD « (17.607 * VM • Y * (PB * PM / 13.6)) / (TM * 060.)
17.607 * 56.951 • 1.003 * ( ?9.72 * .665 / 13.6)
VMSTD s - - 59.821 DSCF
I 02. * 160.)
VOLUME OF NATER VAPOR AT STANDARD CONDITIONS
V*C = .00707 * VLC
VKC = .04707 • 157. = 7.aO SCF
PERCENT MOISTURE IN STACK GAS
BNO = (100. * VHC) / (VMSTD » VHC)
& 100. * 7.00
^ BWO = --— — — — = 11.01 PERCENT
O 59.821 + 7.00
~J
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - BWOJ / 100.
100. - 11.0
FMO = — —— ....... 3 .890
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MD = (PC02 * .00) » (P02 * .32) * (PN2 » PCO) • .28
MO = ( 3.70*40/100) » (11.1*32/100) » ((85.2* .0) * 28/100 = 29.00
MOLECULAR HEIGHT OF STACK GAS
MWS s MD * (1. - (MHO/100)) » 18. * (HhO/100)
MWS = 29.00* (1. -U1.U1/1UU) ) + 18. * (11.01/100) = 27.82
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SORKVH * US + 160.))
VS s 85. 49 * CP * DELP / (SQKT(MwS * PS) * PNTS)
VS = 85.1V * .84 • 82.965 / (SQRT( 27.83 * 29.63) • 12. = 17.29 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
US = VS * AS * 3bUU/laa
OS = 17.29 * 7505. 3600/144 s 3244223. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
QSSTO s 17.647 * OS * PS * (1. - (BMO/100)) / (TS * 460.)
17.647 « 3244223. * 29.63 • (1. - (11.01/100))
QSSTD = —— — ........—.......— z 1588494. SCFH
( 490. * 460.)
>
^ PERCENT ISOKINETIC
o
00 ISO = - (305.58*(TS+460.))«((0.002669«VLC)+(Vf*Y*(PB+(PM/13.6))/(TM«'460.))}/(TT*VS«PS*UN*DN)
(305.58M 490.+ 460.))*((0.002669. 157.)»( 56.951 * 1.003* ( 29.72+( .665/13.6))/( 42.+460.)))
ISO z -. — * U0.2« PERCENT
120. * 17.29 • 29.63 * .404 * .404
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 • MN * 15.43 / VM3TD
CS = 0.001 * .1)000 * 15.43 / 59.821 s .00000 GR/DSCF
PARTICIPATE LBS/HR — EPA METHOD 5
PMR = CS * OSSTO / (15.43 * 453.6)
PMR = .00000 * 1588490. / (15.43 * 453.6) = .00000
-------
Run No. D4.1
3
Sample volume =1.69 m. 59.8? scf
Example calculations
CS (Part) =28.5/1.69=16.9 mg/m3
CS (Part) = 0.001 x28.5 x 15.43/59.82 = 0.007 qr/dscf
CS (S02) =135.6/1.69 = 80.2 mg/m3
= 80.2 x 24.06/61_=_3Jl_ppm
= 0.001 x135.6x 15.43/5aJJ2_sO25_ gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As SO/f
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
28.5
0.0
0.0
0.0
135.6
42.3
3 Concentration,
mg/m
16.9
0.0
0.0
0.0
80.2
25.0
gr/dscf
0.007
0.000
0.000
0.000
0.035
0.011
ppm
30
6
A-409
-------
FIELD DATA
I
M
o
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET «1
SAMPLE TYPE PART/H2SU4/S02
OPERATOR ARMSTRONG
AMBIENT TEMP. (DEC. F) 35.
BAR. PRESS. (IN. HG) 21. 12
STATIC PRESS. (IN. H20) -1.80
FILTER NUMBEH(S) 3530338
STACK INSIDE DIM. (IN) 97. 75 .00
PITOT TUBE COEFF. .84
THERM. NO. 133
LEAKAGE .000 CFM 31 5.
METER CALIB. FACTOR 1.004
READ ft RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60. 0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
r* i n f* v i
LLULK J
943
953
1003
1013
1023
1033
1043
1053
103
113
123
133
143
EVERY 10.0
GAS METtR
READING
(CU.FT.)
537.680
542.190
546.960
551.670
556.500
561.450
566.240
571.140
575.920
580.730
5H5.000
590.670
595.468
MINUTES
VELOCITY
HEAD
(IN.H20)
.047
.050
.048
.050
.053
.049
.052
.048
.050
.051
.056
.050
CLEVELAND OHIU
BATTEHY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.60
.68
.66
.68
.72
.67
.70
.66
.68
.t>9
.76
.68
H20)
ACTUAL
.60
.68
.66
.60
.72
.67
.70
.66
.68
.69
.76
.68
STACK
TEMP
(DEG.F)
487.
495.
507.
474.
485.
496.
483.
499.
510.
474.
482.
490.
DATE 12/12/81
HUN NUMBER D4-2
PROBE LENGTH ft TYPE 4 FOUI GLASS
NOZZLE : I.D. .400
ASSUMED MOISTUHE 13.7
SAMPLE BOX NUMBER
VETE« BOX NUMBER FB/
KETER HEAD OIFF. 1.71
C FACTOR .78
PROBE HEATER SETTING 250.
HEATER BUX SETTING 250.
REFERENCE PRESS. DIFF. .15
DRY GAS METER
TEMP
(DEG.F)
IKLET OUTLET
44. 40.
50. 40.
52. 41.
54. 42.
56. 43.
56. 43.
58. 44.
58. 45.
58. 46.
60. 48.
60. 48.
61. 48.
PUPP
VACUUM
(IN.HG)
2.0
2.2
3.0
3.2
3.5
3.8
3.8
4.0
4.0
4.2
4.0
5.0
SAMPLE
BOX TEMP
(UEG.F)
302.
265.
255.
245.
253.
249.
272.
260.
260.
255.
246.
246.
IPPINGER
TEMP
(OEG.F)
39.
39.
47.
47.
48.
50.
48.
51.
50.
49.
54.
52.
TOTALS
AVERAGE
120.0
•>7.788
.68
.68
490.
56.
44,
3.6 259.
48.
-------
FIELD DATA s RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADEN
REPUBLIC STEEL CLEVELAND OHIO ARMSTRONG
TEST D4-2
STACK OUTLET »1 BATTERY
ENGLISH UNITS
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
12/12/81
943
1143
120.
12
1.
.
.
.
0
004
400 IN
84
68 IN-H20
METRIC UNITS
12/12/Bl
903
1 143
120.
12
1.
10.
•
17.
0
004
2
84
3
ft.
HM-I
VM
TM
VMSTD
VLC
VHC
BWO
FMD
PC02
P02
PCO
PN2
MO
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DHY
MOLECULAR HT-ORY STACK GAS
MOLECULAR hl-STACK GAS
57.788 CU-FT
1.636 CU-M
49.
59.
160.
7.
11.
•
3.
11.
•
85.
29.
27.
8 F
790 SCF
7
564 SCF
23
888
70
10
00
20
04
fiO
9
1
160
11
3
11
85
29
27
.<> C
.693 SCC
.7
.214 SCI"
.23
.888
.70
.10
.00
.20
.04
.80
-------
PB
PSI
PS
TS
VS
AS
USSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE» DRY*
ACTUAL STACK FLOW KATE
PERCENT ISOKINETIC
MG. EPA 5
29.73 IN-MG
-1.20 IN-H20
29.63 IN-HG
090. F
17.3 FPS
7505. SQ-IN
1585051. SCFH
3205338. ACFH
112.6
.0000
.00000 GR/OSCF*
.00000 L8/HH
754.B9 KM-HG
-30.48 KM-H20
752.65 VM-HG
255. C
5.3 KPS
4.842 SU-M
44895. SCPM
91898. ACNH
112.6
.0000
.0000 MG/OSCM
.000 KG/HH
EMISSION RATE
* 66 DEG f, 29.92 IN.HG.
K)
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. oa-2
STACK OUTLET 01 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD = (17.6A7 • VM » Y * (PH » PM / 13.6)) / (TM •» flbO.)
17.617 • 57.788 * 1.U01 * I 29.72 » .682 / 13.6)
VMSTD = — — — «——— ————— — — — — - — — — -. = 59.790 DSCF
I 50. *
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SQRHVH * ITS « «60.))
VS = 85.49 * CP • DELP / ISUKT(MWS • PS) * PNTS)
VS = 85.49 * .84 * 02.958 / (SQRT( 27.BO * 29.63) * 12. = 17.30 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS = VS * AS * 3600/144
CIS = 17.30 » 7505. 3600/144 = 3245338. ACFH
STACK GAS VOLUMETRIC FLOn AT STANDARD CONDITIONS
QSSTU = 17.647 * OS * PS * (1. - (BviU/100)) / (TS * 460.)
17.647 * 3245338. * 29.t,3 * (1. - (11.23/100))
OSSTO s .- — -- — . . ... . = 1585451. SCFH
( 490. * 460.)
PERCENT ISOKINETIC
^ ISO = (305.58«(TS»460.))«((0.002669«VLC)+(VM*Y«(PB*(P*/13.6))/(TM+460.)))/(TT«VS*PS«DN*DN)
I-1
** (305.58*1 490.*4bO.))*((0.002669. 161.)*( 57.788*1.004* ( 29.72*( .682/13.6))/ ( 50.*460.)))
ISO = = 112.61 PERCENT
120. • 17.30 • 29.63 • .400 • .400
PARTICULATE LOADING " EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = U.001 * MN * 15.43 / VMSTD
CS = 0.001 • .0000 • 15.43 / 59.790 = .00000 GR/DSCF
PARTICULAR LBS/HR -- EPA METHOD 5
PMR s CS • OSSTD / (15.43 * 453.6)
PMK = .00000 * 1585451. / (15.43 • 453.6) = .00000
-------
Run No. D4.2
Sample volume = 1.69 m T59.79 scf
Example calculations
CS (Part) = 45.2/ 1.69= 26.7 mg/m3
CS (Part) = 0.001 x 45.2 x 15.43/59.79 = 0.012 qr/dscf
CS (S02) =130.5/1.69 =77.2 mg/m3
=77.2 x 24.06/64 = 29 ppm
= 0.001 x130.5 x 15.43/59.79 = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
45.2
13.5
0.0
0.0
0.9
130.5
15.9
2 Concentration,
mg/m
26.7
8.0
0.0
0.0
0.5
77.2
9.4
gr/dscf
0.012
0.003
0.000
0.000
0.0002
0.034
0.004
ppm
29
2
A-415
-------
FIELD 0»T»
PLANT REPUBLIC STEtL
SAMPLING LOCATION STACK OUTLET »1
SAMPLE TYPE PART/H2S04/S02
OPERATOR DAN FITZGtRALO
AMBIENT TEMP. (DEG.F) 35.
BAR. PRESS. (IN.HG) 29.72
STATIC PRESS. (IN. M20) -1.20
FILTER NUMBERU) 3530087
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .84
THERM. NO. 133
LEAKAGE .007 CFM S 6.
METER CALIB. FACTOR .982
READ & RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
940
950
1000
1010
1020
1030
1040
1050
1100
1110
1120
1130
1140
EVERY 10. 0
GAS METER
READING
(CU.FT.)
804.107
808.315
812.330
816.380
820.675
825.190
829.340
833.740
837.945
842.280
846.560
851.145
855.456
MINUTES
VELOCITY
HEAD
(IN.H20)
.047
.050
.048
.050
.053
.049
.052
.048
.050
.051
.056
.050
CLEVELAND OHIO
BATTERY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.59
.62
.59
.63
.66
.61
.65
.59
.61
.64
.70
.62
H20)
ACTUAL
.59
.62
.59
.63
.66
.61
.65
.59
.61
.64
.70
.62
STACK
TEMP
(DEG.F)
487.
495.
507.
474.
485.
496.
4B3.
499.
510.
494.
482.
490.
DATE 12/12/81
RUN NUMBER 1)4-3
PROBE LENGTH « TYPE 4 FOUT GLASS
NOZZLE : I.D. .404
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
METER BOX NUMBER FB8
MF.TER HEAD OIFF. 1.91
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
K FACTOR 11856.2
DRY GAS
METER
TEMP
(DEC
INLET
38.
43.
46.
47.
48.
49.
50.
50.
50.
52.
54.
56.
.F)
OUTLET
37.
37.
38.
38.
39.
40.
40.
41.
42.
43.
44.
46.
PUMP
VACUUM
(IN.HG)
2.5
3.0
4.0
4.5
5.0
5.0
5.0
5.0
5.0
5.5
5.5
5.0
SAMPLE
BOX TEMP
(DFG.F)
410.
406.
405.
405.
402.
408.
416.
411.
415.
412.
413.
410.
IMPINGER
TEMP
(DEG.F)
42.
43.
43.
44.
44.
47.
50.
51.
52.
52.
53.
53.
TOTALS
AVERAGE
120.0
51.349
.63
.63
492.
49.
40.
4.6
409,
48.
-------
PARTICIPATE FIELD DATA « RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST D4-3
STACK OUTLET #1 BATTERY
ENGLISH UNITS
TEST DATE 12/12/61
TB
TF
TT
NP
Y
ON
CP
TIME-START 940
TIME-FINISH 1140
NET TIME OF TEST, MIN. 120.0
NET SAMPLING POINTS 12
METER CALIBRATION FACTOR .982
SAMPLING NOZZLE DIAMETER .404 IN
PITOT TUBE COEFFICIENT .64
METRIC UNITS
12/12/81
940
1140
120.0
12
.902
10.3 KM
.64
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS ANQ SILICA GEL,ML.
VNC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR HT-ORY STACK GAS
MHS MOLECULAR WT-STACK GAS
.63 IN-H20
51.349 CU-FT
44.5 f
52.502 SCF
149.3
7.028 SCF
11.81
.H82
3.70
11.10
.00
85.20
29.04
27.73
15.9 KM-H20
1.454 CU-M
6.9 C
1.487 SCM
149.3
.199
11.81
.882
3.70
11.10
.00
65.20
29.04
27.73
-------
PB
PS1
P3
TS
VS
AS
QSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES. ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLO* RATEr DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
M6. EPA 5
EMISSION RATE
* 68 DEC F, 29.9? IN.HG.
89.78 IN-MG
-1.20 IN-H20
89.63 IN-HG
098. F
17.3 FPS
7505. SO-IN
1575619. SCFH
3851926. ACFH
97.5
.0000
.00000 GR/DSCF*
.00000 LB/HR
750.89 ffc-HG
-30.08 VM-H80
758.65 *M-HG
855. C
5.3 *PS
q.eoa SQ-M
04617. SCCH
98085. ACVH
97.5
.0000
.0000 MG/OSCM
.000 KG/HR
I
^
M
00
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. na-3
STACK OUTLET 01 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO * (17.647 • VM * Y * (PB » PM / 13.6)) / (TM * 460.)
17.647 * SI.349 * .982 * ( 29.72 » .626 / 13.6)
VMSTD » ————— — — ............... ... ... = 52.502 DSCF
I 45. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC * .04707 • VLC
VNC * .04707 • 149. = 7.03 SCF
PERCENT MOISTURE IN STACK GAS
BNO 3 (100. * VHC) / (VMSTD » VWC)
100. • 7.03
> BNO « • = 11.81 PERCENT
^ 52.502 * 7.03
M
U3
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - BNO) / 100.
100. - 11.8
FMD « ———————— * .882
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD » (PC02 • .44) * (P02 * .32) * (PN2 » PCO) * .28
MO = ( 3.70*44/100) * (11.1*32/100) * ((85.2* .0) * 28/100 = 29.04
MOLECULAR NEIGHT OF STACK GAS
MNS = MO * (1. - (BNO/100)) + 18. * (BWU/100)
MHS * 29.04* (1. -(11.81/100)) * 18. * (11.81/100) * 27.73
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP » SUM. OF THE 3QRHVH * (T3 » 460.))
VS * 85.49 • CP * OELP / (SOHT(MNS * PS) • PNTS)
VS = 85.49 * .84 * 83.031 / (SQRT( 27.73 • 89.63) * 12. = 17.33 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS s VS * AS * 3600/140
OS * 17.33 * 7505. 3600/144 : 3251926. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD * 17.647 * OS * PS * (1. - (BWO/100)) / (TS * 460.)
17.647 * 3251926. * 29.63 * (1. - (11.81/100))
OSSTD = ——— —— -- ———— — . . ...... = 1575619. SCFH
( 492. » 460.)
> PERCENT ISOKINETIC
4^
to ISO = (305.58*(TS+4t>0.))*((0.002669*VLC)+(VM*Y*(PB»(PM/13.6)) /(TM«460.)))/(TT*V3*PS*DN*DN)
o
(305.58*( 492.+460.))*((0.002669* 149.)+( 51.349* .982M 29.72+( .626/13.6))/( 45.+460.)))
ISO 3 . — s 97.54 PERCENT
120. * 17.33 * 29.63 * .404 * .404
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS s 0.001 * MN * 15.43 / VMSTO
CS a 0.001 * .0000 • 15.43 / 52.502 = .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR * CS * OSSTO / 115.43 * 453.6)
PMR = .00000 * 1575619. / (15.43 * 453.6) = .00000
-------
Run No.04.3
Sample volume = 1.49 m3T52.50 scf
Example calculations
CS (Part) =24.8 /I.49 = 16.6 mg/m3
CS (Part) = 0.001 x 24.8 x 15.43/52.50 = 0.007 qr/dscf
CS (S02) =118.3/1.49 = 79.4 mq/m3
= 79.4 x 24.06/64 = 30 ppm
= 0.001 x118.3 x 15.43/52.50 = Q.Q35 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
24.8
0.7
0.9
3.2
118.3
6.7
3 Concentration,
mg/m
16.6
0.5
0.6
2.1
79.4
4.5
gr/dscf
0.007
0.0002
0.0003
0.0001
0.035
0.002
ppm
30
1
A-421
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND
COKE STACK
M5-250
DO
35.
29.72
-1.20
3530320
97.50 .00
.63
.000 CFM a
.992
3.0 IN.HG
READ » RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
CLOCK)
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H2U)
ORIFICE PRESSURE STACK
DIFFERENTIAL TEMP
(IN.H20) (DEG.F)
DATE 12/12/B1
RUN NUMBER 01-5
PROBE LENGTH ft TYPE 5' GLASS
N02ZLE : I.D. .431
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
METER BOX NUMBER FBI
METER HEAD OIFF. 1.87
C FACTOR .71
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .13
DESIRED
ACTUAL
DRY GAS METER
TEMP
(DEG.F)
II^LET OUTLET
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(OEG.F)
IMPINGER
TEMP
(DEG.F)
INIT
£>
Ni
TOTALS
AVERAGE
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
120.0
940
950
1000
1010
1020
1030
1040
1050
1100
1110
1120
1130
1140
72.306
77.320
82.320
87.250
92.220
97.240
102.260
107.290
112.340
117.400
122.400
127.520
132.653
60.347
.055
.055
.055
.055
.055
.055
.055
.055
.055
.055
.055
.055
.81
.81
.81
.81
.»!
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
.81
487.
495,
507.
474,
485.
496,
483,
499.
510,
474,
482,
490,
490,
40.
43.
49.
54.
57.
59.
61.
62.
63.
63.
64.
65.
57.
35.
35.
36.
38.
40.
41.
43.
44.
45.
46.
47.
47.
41,
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.1
2.1
2.1
2.2
2.2
2.1
256.
283.
249.
265.
280.
246.
237.
286.
249.
233.
298.
269.
263.
40.
42.
42.
44.
44.
46.
46.
46.
48.
48.
48.
48.
45.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO
TEST 04-5
COKE STACK
NJ
U)
TEST DATE
TB TIME-START
TF TIME-FINISH
TT NET TIME OF TEST, MIN.
NP NET SAMPLING POINTS
Y METER CALIBRATION FACTOR
DN SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL MZO COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VNC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BWO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC03 PERCENT CO? BY VOL., DRY
P03 PERCENT 03 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT Ni BY VOL., DRY
MD MOLECULAR HT-ORY STACK GAS
MWS MOLECULAR XT-STACK GAS
ENGLISH UNITS
12/12/81
940
1140
120.0
12
.992
.431 IH
.83
.81 IN-H20
bO.347 CU-FT
49.0 F
61.B02 SCF
176.6
fl.313 SCF
11.86
.881
3.70
11.10
.00
85.20
89.04
37.73
METRIC UNITS
12/12/81
940
1140
120.0
12
.992
10.9
.83
20.6
1.709
9.5
1.750
176.6
.235
11.86
.881
3.70
11.10
.00
85.20
29.04
27.73
KM
PM-H20
CU-M
c
sec
SCM
-------
PB
PSI
PS
TS
VS
A3
QSSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, A8S.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLON RATE, DRY*
ACTUAL STACK FLO" RATE
PERCENT ISOKINETIC
MG. EPA 5
29.72 IN-HG
-1.20 IN-M20
29.63 IN-HG
090. F
17.9 FPS
7466. SO-IN
1620395. SCFM
3300189. ACFH
97.6
.0000
.00000 GR/DSCF*
.00000 LB/HR
754.89 PM-HG
-30.48 VM-H20
752.h5 HM-HG
255. C
5.5 *PS
4.817 SO-H
45882. SCKH
94564. ACNH
97.6
.0000
.0000 MG/DSCM
.000 KG/HR
EMISSION RATE
* 68 DEC F, 29.42 IN.HG.
**
to
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. D4-5
COKE STACK
VOLUME OF DRY 6AS SAMPLED AT STANDARD CONDITIONS
VM3TD » (17.647 * VM • Y • (PB * PM / 13.6)) / (TM «• 460.)
17.647 * 60.347 * .993 * ( 39.78 » .810 / 13.6)
VMSTO B ——— — —— . —.... ... . —... * 61.803 DSCF
I 49. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC a .04707 • VLC
VMC * .04707 * 177. = 8.31 SCF
PERCENT MOISTURE IN STACK GAS
BMO a (100. • VMC) / (VMSTD » VMC)
!f 100. • 8.31
^ BMO = = 11.86 PERCENT
K> 61.802 * 8.31
cn
MOLE FRACTION OF DRY STACK GAS
FMD = (100. > BMO) / 100.
100. - 11.9
FMD s ————————— s .881
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MO a (PC03 * .44) * (P03 * .33) * (PN3 * PCO) • .38
MO = ( 3.70*44/100) + (11.1*33/100) * ((85.?+ .0) * 38/100 = 39.04
MOLECULAR HEIGHT OF STACK GAS
MNS ' MD * (1. - (BMU/100)) + 18. • (BWO/100)
MM3 = 39.04* (1. .(11.86/100)) + 18. * (11.86/100) * 37.73
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SORHVH * (T3 * 460.))
VS = 85.49 • CP * DELP / (SO«T(MNS * PS) * PNTS)
VS = 85.49 * .83 * 86.747 / ISORT( 27.73 * 39.63) • 12. = 17.90 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
03 = VS * AS * 3600/144
OS * 17.90 * 7466. 3600/144 * 3340189. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD « 17.647 * OS • PS • (1. - (BWO/100)) / (TS * 460.)
17.647 * 3340189. • 29.63 * (1. - (11.86/100))
OSSTD = = 1620295. SCFH
( 490. * 460.)
jp PERCENT ISOKINETIC
I
*• ISO s (305.5B*(TS*460.))*((0.002669*VLC)*(VM*Y*(PB'»(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN*DN)
NJ
^ (305.5B*( 090.+460.))*((0.002669* 177.)*( 60.347* .992*1 29.72*( .810/13.6))/C 49.»460.)))
ISO a .....-..........-.._-...............................—........................................... = 97.60 PERCENT
120. * 17.90 • 29.63 • .431 * .431
PARTICULATE LOADING -- EPA METHOD 5 (AT STANDARD CONDITIONS)
CS e 0.001 * MN • 15.43 / VMSTD
C3 z 0.001 * .0000 * 15.43 / 61.802 = .00000 GR/DSCF
PARTICULATE L8S/HR — EPA METHOD 5
PMR c CS * OSSTD / (15.43 • 453.6)
PMR c .00000 * 1620295. / (15.43 * 453.6) = .00000
-------
Run No. D4.5
•3
Sample volume = 1.75m T 61.80 scf
Example calculations
CS (Part) =31.2/1.75=17.8 mq/m3
CS (Part) = 0.001 x31.2 x 15.43/61-8 = 0.008 qr/dscf
3
CS (S02) = / = mg/nT
= x 24.06/ = ppm
= 0.001 x x 15.43/
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
31.2
21.7
20.2
15.1
14.9
12.3
0.0
0.0
0.0
84.5
2.9
8.5
o Concentration,
mg/m
17.8
12.4
11.5
8.6
8.5
7.0
0.0
0.0
0.0
48.3
1.6
4.8
gr/dscf
0.008
0.005
0.005
0.004
0.004
0.003
V
0.000
0.000
0.000
0.021
0.0007
0.002
ppm
A-427
-------
FIEtD DATA
to
CO
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKt STACK
SAMPLE TYPE M8-bOO
OPERATOR 00
AMBIENT TEMP.(OEG.F) 35.
bAR. PRESS. (IN. HG) 29.72
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530226
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .63
THERM. NO.
LEAKAGE .000 CFM a 12.
METER CALIB. FACTOR .967
READ ft RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(WIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
60.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
n or tt \
I-UUIK I
942
952
1002
1012
1022
1032
1042
1052
1102
1112
1122
1132
1142
EVERY 10.0
GAS METER
READING
ICU.FT.)
621.607
626.570
631.360
636.160
841.040
845.910
850.750
855.560
860.440
865.290
670.160
875.100
680.060
MINUTES
VELOCITY
HEAD
(IN.H20)
.055
.055
.055
.055
.055
.055
.055
.055
.055
.055
.055
.055
CLEVELAND OHIO
5 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.58
.58
.56
.58
.58
.58
.56
.58
.56
.58
.58
.58
H20)
ACTUAL
.58
.58
.56
.58
.58
.58
.58
.58
.56
.58
.58
.58
STACK
TEMP
(DEG.F)
487.
495.
507.
474.
485.
496.
463.
499.
510.
474.
482.
490.
DATE 12/12/81
RUN NUMBER D4-b
PROBE LENGTH * TYPE 4* GLASS
NOZZLE : I.U. .378
ASSUMED MOlSTUhfc 13.7
SAMPLE BOX NUMBER
METER BOX NUMBER FBb
METEN HEAD DIFF. 1.51
C FACTOR .90
PROBt HEATER SETTING bOO.
HEATER BUX SETTING bOO.
REFERENCE PRESS. OIFF. .16
DRY GAS
METER
TEMP
(DEG
INLET
35.
37.
40.
44.
47.
48.
50.
50.
50.
50.
51.
51.
.F)
OUTLET
38.
36.
38.
38.
39.
39.
40.
40.
40.
42.
42.
43.
PUMP
VACUUM
(IN.H6)
4.0
5.6
7.3
7.8
7.9
6.2
9.3
10.2
10.9
11.3
11.6
11.6
SAMPLE
BOX TEMP
(DEG.F)
543.
585.
599.
646.
633.
620,
625.
634.
636.
637.
628.
617.
IMPINGER
TEMP
(DEG.F)
37.
38.
36.
36.
40.
40.
42.
42.
44.
44.
46.
48.
TOTALS
AVERAGE
120.0
58.273
.56
.58
490.
46.
40.
8.6 617.
41,
-------
PARTICULATE FIELD DATA & RtSIILTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DO
TEST D4-6
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
DN
CP
PM
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
942
1142
120
12
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL.ML.
Vt«C VOLUME OF WATER VAPOR
AT STANDARD CONDITIONS*
BHO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.. DRY
P02 PERCENT 02 BY VOL.. DRY
PCO PERCENT CO BY VOL.. DRY
PN2 PERCENT N2 MY VOL.. DRY
Ml) MOLECULAR HT-DRY STACK GAS
MWS MOLECULAR WT-STACK GAS
ENGLISH UNITS
12/12/61
942
1142
120.0
12
.967
.378 IN
.63
.58 IN-H20
58.273 CU-FT
42.9 F
58.849 SCF
160.0
7.531 SCF
11.35
.687
3.70
11.10
.00
65.20
29.04
27.78
METRIC UNITS
12/12/81
1142
120.0
12
.967
9.6
.83
14.7
1.650
6.1
1.666
160.0
.213
11.35
.887
3.70
11.10
.00
85.20
29.04
27.78
CM
CM-H
CU-M
C
sec
sec
-------
PB
PSI
PS
TS
VS
A3
OSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE, DRY*
ACTUAL STACK FLON RATE
PERCENT ISOKINEUC
MG. EPA 5
29.72 IN-HG
-1.20 IN-H20
29.63 IN-HG
q. ACFH
120.3
.0000
.00000 GR/OSCF*
.00000 L8/MR
750.89 f'M-HG
•30.18 H
752.65 HM-HG
255. C
5.a fPS
a.817 SO-M
46101. 3CKH
9
-------
EXAMPLE PAHTICULATE CALCULATIONS TEST NO. Do-6
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO * (17.647 • VM * Y * (PB * PM / 13.6)) / ITM «• 060.)
17.607 * 58.273 * .967 • ( 29.7? * .580 / 13.6)
VMSTO = --—-- — - --------- — ------ - ----- ......... — ........ = 38.809 OSCF
( 03. » 060.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC = .00707 * VLC
VMC = .00707 * 160. = 7.53 SCF
PERCENT MOISTURE IN STACK GAS
BMO = 1100. * VHC) / (VMSTD + VMC)
100. * 7.53
> BMO a ............ ---- — — ...... = 11.35 PERCENT
i, 58.849 * 7.53
U)
I-1
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - BMO) / 100.
100. > 11.3
..... ......... r ,»B7
100.
AVERAGE MOLECULAR MEIGHT OF DRY STACK GAS
MD = (PC02 * .00) + (P02 * .32) * (PN2 » PCO) * .28
MD = ( 3.70*00/100) *• (11.1*32/100) * ((85. 2*-. 0) * 28/100 = 29.00
MOLECULAR MEIGHT OF STACK GAS
MMS = MD • (1. - (BWO/100)) * 18. * (BWO/IOO)
MMS * 29.00* (1. -(11.35/100)) * 18. * (11.35/100) = 27.78
-------
N)
STACK 6*3 VELOCITY AT STACK CONDITIONS
OELP a SUM. OF THE SQRMVH * (TS » 060.))
VS = 85.19 • CP * OELP / (SQRT(MHS * PS) * PNTS)
VS = 85.49 * .85 * 86.747 / (S(jHT( 27.78 • £9.63) * 12. = 17.88 FPS
STACK GAS VOLUMETRIC FLOH AT STACK CONDITIONS
OS = VS * AS * 3600/144
OS = 17.88 * 7466. 3600/144 = 3336804. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTO « 17.647 • OS * PS • (1. • (BNO/100)) / (TS » 460.)
17.647 • 3336804. * 29.63 * (I. - (11.35/100))
OSSTO = ------------------------------ — — ----------------- = 1628021. SCFH
( 490. * 460.)
PERCENT ISOKINETIC
ISO = (305.58*(TS+460.))*((0.002669*VLC)+(V»«*Y«(PB«(PM/13.6))/(TM»460.)))/(TT*VS*PS*DN*DN)
(305.58*t 490. «460.))*((0. 002669* 160. )*( 58.273* .967*1 29.72M .580/1 3.6) )/( 43. +460.)))
ISO x ----------------------------------------- — ------------------------ — --- - ----------------------- « 120.26 PERCENT
120. * 17.88 * 29.63 * .378 * .378
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 * MN * 15.43 / VMSTD
CS = 0.001 * .0000 * 15.43 / 58.849 = .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR s CS * OSSTD / (15.43 • 453.6)
PMR = .00000 * 1628021. / (15.43 * 453.6) * .00000
-------
Run No. D4.6
3
Sample volume = 1.67 m , 58.85 scf
Example calculations
CS (Part) =17.5 /I.67 = 10.5 ma/m3
CS (Part) = 0.001 x 17.5 x 15.43/58.85 = 0.004 qr/dscf
CS (S02) = 90.1/1.67 = 54.0 ma/m3
= 54.0 x 24.06/64 = 20 ppm
= 0.001 x 90.1 x 15.43/58.58 = D.n?4 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H2S04
As H2S04.2H20
Water soluble sulfates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
17.5
0.0
0.0
0.0
90.1
74.7
2 Concentration,
mg/m
10.5
0.0
0.0
0.0
54.0
44.7
\
gr/dscf
0.004
0.000
0.000
0.000
0.024
0.020
ppm
20
11
A-433
-------
FIELD D»TA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEC.F)
BAR.PRESS.(IN.H6)
STATIC PRESS.(IN.H80)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND OHIO
STACK OUTLET «1 BATTERY
PART/H8S04/S08
36.
89.78
-1.20
3530185
97.75 .00
.ea
133
.016 CFM a 5.5 IN.HG
1.003
READ » RECORD DATA EVERY 10.0 MINUTES
DATE
RUN NUMBER
PROBE LENGTH ft TYPE
NOZZLE : I.U.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER
METER HEAD DIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
05-1
5 FOOT GLASS
.401
13.7
FB8
1.76
850.
850.
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(84-HR
n fir* i
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H80)
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H80)
DESIRED ACTUAL
STACK
TEMP
(DEG.F)
DRY GAS METER
TEMP
(DEG.F)
IKLET OUTLET
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPINGEH
TEMP
(DEG.F)
INIT
.to.
CO
TOTALS
AVERAGE
o
10.0
80.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
180.0
180.0
1404
1414
1484
1434
1444
1454
1504
1514
1584
1534
1544
1554
1604
469.955
474.660
479.410
484.430
489.310
49q,080
498.750
503.500
508.450
513.390
518.450
583.300
588.833
58.878
.050
.058
.057
.055
.050
,050
.050
.055
.055
.055
.055
.055
.66
.68
.75
.78
.66
.66
.66
.78
.78
.78
.78
.78
.70
.66
.68
.75
.78
.66
.66
.66
.78
.78
.78
.78
.78
500.
458.
465.
476.
458.
477.
490.
458.
465.
476.
458.
477.
.70 471.
38.
40.
41.
44.
44.
43.
46.
46.
46.
46.
46.
46.
44.
38.
40.
40.
40.
40.
40.
40.
40.
40.
40.
40.
40.
40.
8.0
8.0
8.5
3.0
3.8
3.9
4.8
4.4
4.4
4.5
4.8
5.0
851,
846,
875.
859,
847,
858,
848.
860.
844.
854,
858.
845,
3.7 853.
56.
56.
45.
45.
47.
49.
50.
56.
56.
57.
68.
57.
53.
-------
PAHTICULATE FIELD DMA s RESULTS TABULATION
> NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO
TEST 05-1
STACK OUTLET «1 BATTERY
U)
TEST DATE
TB TIME-START
TF TIME-FINISH
TT NET TIME OF TEST, M1N.
NP NET SAMPLING POINTS
Y METER CALIBRATION FACTOR
ON SAMPLING NOZZLE DIAMETER
CP PITOT TUBE COEFFICIENT
PM AVERAGE ORIFICE PRESSURE
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL HZO COLLECTED IN
IMPINGERS AND SILICA GELpML.
VWC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BWO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT COa BY VOL.. DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL.. DRY
MO MOLECULAR NT-DRY STACK GAS
MNS MOLECULAR MT-STACK GAS
ENGLISH UNITS
12/12/81
1000
1600
120.0
12
1.003
.001 IN
.80
.70 IN-H20
SB. 278 CU-FT
01.9 F
61.308 SCF
170.9
8.233 SCF
11.80
.882
3.70
11.80
.00
80.50
29.06
27.75
METRIC UNITS
12/12/81
1000
1600
120.0
12
1.003
10.2
.80
17.8
1.650
5.5
1.736
170.9
.233
11.80
.882
3.70
11.80
.00
80.50
29.06
27.75
MM
MM-H20
CU-M
C
SCI*
SCM
-------
PB
PSI
P3
TS
VS
AS
OSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ASS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE» DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
EMISSION RATE
• 68 DEG F, 29.92 IN.HG.
£9.78 IM-HG
-1.20 IN-H20
29.69 IN-HG
«71. F
17.6 FPS
7505. SO-IN
1639020. SCFM
3303306. ACFH
111.1
.0000
.00000 GR/DSCF*
.00000 LB/HR
756.11 PM-HG
-30.48 ^
750.17 »»-HG
200. C
5.a VPS
4.802 SO-M
4b012. SC»*H
93500. »CHH
111.1
.0000
.0000 MG/DSCM
.000 KG/HR
*»
U)
-------
EXAMPLE PARTICULATE CALCULATIONS TFST NO. D5-1
STACK OUTLET *1 BATTEkY
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VMSTD = (IT. 647 * VM * Y • (PB * PM / 13.6)) / (TM * 460.)
17.647 • 56.278 * 1.003 * ( 29.78 * .699 / 13.6)
VMSTD = —————— — — -- — -- --- ---. --- - — . ---- . ------- = 61.308 DSCF
( ag. + 060.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC a .04707 • VLC
VHC » .04707 * 175. a 8.23 SCF
PERCENT MOISTURE IN STACK GAS
BHO • (100. * VNC) / (VMSTD * VMC)
100. * 8.23
•y BHO a — — — — - — — — — s 11.84 PERCENT
I 61.308 «• B.23
U)
-J
MOLE FRACTION OF DRT STACK GAS
FMO > (100. - BWO) / 100.
100. - 11.8
FMD a — ... ---- - -------- = .882
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD a (PC02 • ,4fl) * (P02 * .32) * (PN2 * PCD) • .28
MD * ( 3.70*44/100) » (11.8*32/100) + ((84.5* .0) * 28/100 = 29.06
MOLECULAR HEIGHT OF STACK GAS
MHS = MU * (1. • (BMO/100)) * 18. * (BWO/100)
MMS = 29.06* (1. -(11.84/100)) » 18. * (11.8Q/100) s 27.75
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP * SUM. OF THE SORUVH * ITS * 160.))
VS a 85.09 • CP * DELP / ISQRT(MWS • PS) * PNTS)
VS » 85.49 * .84 * 84.461 / (SORT( 27.75 * 39.69) • 18. = 17.61 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS = VS * AS * 3600/144
OS = 17.61 * 7505. 3600/144 = 3303306. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD « 17.647 • OS • PS • (1. - (BwO/100)) / (TS * 460.)
17.647 * 3303306. * 29.69 * (1. - (11.84/100))
OSSTD = — —————— — — -—............. = 1639084. SCFH
( 471. «• 460.)
>
I PERCENT ISOKINETIC
>t*
ro ISO = (305.58*(T3+460.))*((0.002669*VLC)*(VM*Y*(PB«(PM/13.6))/(TM*460.)))/(TT*VS*PS«DN*ON)
(305.58*( 471.»460.))*((0.002669* 175.)*( 58.278*1.003*( 29.78*( .699/13.6))/( 48.»460.)))
130 s . = 111.14 PERCENT
120. * 17.61 * 29.69 * .401 * .401
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
CS = 0.001 * .0000 * 15.43 / 61.300 = .00000 GR/DSCF
PARTICULATE L8S/HR — EPA METHOD 5
PMR = CS * OSSTD / (15.43 * 453.6)
PHR B .00000 * 1639024. / (15.43 * 453.6) = .00000
-------
Run No. D5.1
Sample volume = 1.74 m , 61.31 scf
Example calculations
CS (Part) = 23.3/1.74 = 13.4 mq/m3
CS (Part) = 0.001 x 23.3 x 15.43/61.31 = 0.006 qr/dscf
CS (S02) =131.8/1.74 = 75.7 ma/m3
= 75.7 x 24.067 64 = 28 ppm
= 0.001 X131.8 x 15.43/61.31 = 0.033 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
23.3
3.4
4.6
3.7
131.8
8.8
- Concentration,
mg/m
13.4
1.9
2.6
2.1
75.7
5.0
gr/dscf
0.006
0.001
0.001
0.001
0.033
0.002
ppm
28
1
A-439
-------
FIELD 0»T*
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(OEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEEL CLEVELAND OHIO
STACK OUTLET «1 BATTERY
PART
36.
39.78
•1.20
97.75
.84
133
.000 CFM a
1.004
.00
4.0 IN.HG
READ & RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
CLOCK)
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE STACK
DIFFERENTIAL TE"P
(IN.H20) (DEG.F)
DESIRED ACTUAL
DATE
RUN NUPBER
PHOBE LENGTH * TYPE
NOZZLE : 1.0.
ASSUMED MOISTURE
SAKPLE BOX NUMBER
PETER BOX NUMBER
*ETER HF»0 DIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
12/12/81
05-2
4 FUOT GLASS
.401
13.7
FB7
1.71
250.
250.
DRY GAS METER PUMP SAMPLE IMPINGER
TEMP VACUUM BOX TEMP TEMP
(DEG.F) (IN.HG) (DEG.F) (DEG.F)
INLET OUTLET
INIT
>t^
£>
o
TOTALS
AVERAGE
o
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
120.0
1407
1417
1427
1437
1447
1457
1507
1517
1527
1537
1547
1557
1607
595.690
600.660
605.520
610.640
615.630
620.450
625.280
630.080
635.100
640.150
645.170
650.210
655.250
59.360
.050
.052
.057
.055
.050
.050
.050
.055
.055
.055
.055
.055
.68
.70
.77
.74
.68
.68
.68
.74
.74
.74
.74
.74
.72
.68
.70
.77
.74
.68
.68
.68
.74
.74
.74
.74
.74
.72
500,
458.
465,
476.
452.
477,
490,
458.
465.
476.
458.
477,
471,
46.
47,
50,
53,
56,
57,
58,
60,
60,
60,
60,
60.
56.
44.
44.
44.
44.
45.
45.
46.
46.
47.
48.
48.
48.
46.
1.0
1.5
1.5
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
260.
252.
288.
269.
246.
260.
248.
270.
250.
260.
270.
261.
1.8 261.
46.
46.
47.
47.
49.
51.
47.
55.
53.
59.
59.
40.
50.
-------
PARTICIPATE FIELD DATA * RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO
TEST D5-2
STACK OUTLET «1 BATTERY
TEST
TB
TF
TT
NP
Y
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MlN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
ENGLISH UNITS
12/12/81
1407
1607
120.0
12
1.004
.401 IN
.P4
.72 IN-H20
METRIC UNITS
12/12/81
1407
1607
120.0
12
1.004
10.2 MM
.84
18.3 PM-I
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VMC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
BKO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRV
P02 PERCENT 02 BY VOL.. DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR WT-ORY STACK GAS
MWS MOLECULAR HT-STACK GAS
59.360 CU-FT
50.7 F
61.441 SCF
186.0
8.755 SCF
1.681 CU-M
10.4 C
1.740 SCM
186.0
.248 SCK
12.47
.875
3.70
11.80
.00
84. bO
29.06
27.68
12.47
.875
3.70
11.80
.00
84.50
29.06
27.68
-------
PB
PSI
PS
TS
VS
AS
OSSTO
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATEr DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
29.78 IN-HG
-1.20 IN-H20
29.69 IN-HG
a?t. F
17.6 FP3
7505. SO-IN
1629300. SCFH
3307486. ACFH
112.0
.0000
.00000 GR/OSCF*
.00000 LB/HR
756.41 MM-HG
-30.48 MM-H20
750.17 VM-HG
2«4. C
5.4 CPS
4.842 SO-M
16137. SCMH
93658. »CVH
112.0
.0000
.0000 MG/OSCM
.000 KG/HR
EMISSION RATE
* 68 OEG F, 29.92 IN.HG.
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. D5-2
STACK OUTLET «1 BATTERY
VOLUME OF DRV GAS SAMPLED AT STANDARD CONDITIONS
VM3TD * (17.607 * VM • Y * (PB * PM / 13.6)) / (TM •» 060.)
17.607 * 59.360 • 1.000 * ( 29.78 + .719 / 13.6)
VMSTO s ........... ........ . . ..... . s 61.001 DSCF
( 51. * 060.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VHC s .00707 * VLC
VMC * .00707 * 186. 3 8.76 SCF
PERCENT MOISTURE IN STACK GAS
BNO s (100. • VhC) / (VMSTO «• VHC)
•f 100. • 8.76
** BMO = s 12.07 PERCENT
*> 61.001 * 8.76
OJ
MOLE FRACTION OF DRY STACK GAS
FMD » (100. - BMU) / 100.
100. - 12.5
FMD s ———————— a .875
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO s (PC02 • .00) * (PU2 * .32) * (PN2 * PCO) * .28
MD 3 ( 3.70*00/100) » (11.8*32/100) * ((80.5* .0) • 28/100 = 29.06
MOLECULAR HEIGHT OF STACK GAS
MMS s MD * (1. - (BHO/10U)) + 18. * (RWO/100)
MHS * 29.06* (1. -(12.07/100)) + 18. * (12.07/100) = 27.68
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP s SUM. OF THE SQRT(VH * (TS « 460.))
VS > 85.49 * CP * DELP / (SQRT(MMS * PS) * PNTS)
VS = 85.49 * .84 • 84.461 / (SORT( 27.68 * 29.69) * 12. = 17.63 FPS
STACK GAS VOLUMETRIC FLON AT STACK CONDITIONS
OS = VS * AS * 3600/144
OS > 17.63 * 7505. 3600/144 x 3307488. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD a 17.647 * OS * PS * (1. - (BNO/100)) / (TS » 460.)
17.647 * 3307488. • 29.69 • (1. - (12.47/100))
OSSTD « ——————-- ——— — .---- —............ . s 1629300. SCFH
( 471. * 460.)
PERCENT ISOKINETIC
ISO * (305.58*(TS*46U.))*((0.002669*VLC)*(VM*Y*(PB»(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN«DN)
(305.58*( 471.+460.))*((0.002669* 186.)*( 59.360*1.000*( 29.78*1 .719/13.6))/( 5t.*460.)))
ISO 9 — . —. ..... — ......... ........ s 112.05 PERCENT
120. * 17.63 * 29.69 * .401 * .401
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTD
CS « 0.001 * .0000 * 15.43 / 61.441 = .00000 GR/DSCF
PARTICULATE LBS/HR « EPA METHOD 5
PMR s CS * OSSTD / (15.43 * 453.6)
PMR a .00000 * 1629300. / (15.43 * 453.6) * .00000
-------
Run No. D5.2
Sample volume = 1.74 m3.61.44 scf
Example calculations
CS (Part) = 20.0/1.74 = 11.5 mg/m3
CS (Part) = 0.001 x 20.0 x 15.43/61.44 = 0.005 qr/dscf
CS (S02) = /.
. mg/m*
x 24.06/_
.ppm
= 0.001 x
.x 15.43/.
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
20.0
8.7
0.8
1.1
1.7
74.5
0.7
202
2 Concentration,
mg/m
11.5
5.0
0.5
0.6
1.0
42.8
0.40
116
gr/dscf
0.005
0.002
0.0002
0.0003
0.0004
0.019
0.0002
0.05
ppm
I PA contaminated
A-445
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEG.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBEft(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEtL CLEVELAND OHIO
STACK OUTLET «1 BATTERY
PARTICULATE/SU2
DAN FITZGERALD
36.
29.78
-1.20
3530323
97.75 .00
.84
133
.014 CFM 9 11.0 IN.HG
.982
READ S RECORD DAT* EVERY 10.0 MINUTES
DATE
RUN NUMBER
PROBE LENGTH ft TYPE
NOZZLE : I.D.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
PETER BOX NUMBER
*ETE« HEAD OIFF.
PROBE HEATER SETTING
HEATER BOX SETTING
K FACTOR
12/12/81
05-3
4 FOOT GLASS
.402
13.7
F8B
1.91
350.
350.
11856.2
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
ri nric i
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H2U)
DESIRED ACTUAL
STACK
TE"P
(DEG.F)
DRY GAS METER
TEMP
(DEG.F)
IKLET OUTLET
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(OEG.F)
IMPINGEH
TEMP
(DEG.F)
INIT
CTi
TOTALS
AVERAGE
o
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
120.0
1358
1408
1418
1428
1438
1448
1458
1508
1518
1528
1538
1548
1558
8S6.004
860.320
864.760
869.320
673.935
878.410
883.170
887.660
892.255
896.900
901.340
905.770
910.397
54.393
.050
.055
.055
.055
.050
.057
.055
.055
.055
.050
.052
.057
.62
.71
.70
.70
.65
.72
.69
.71
.70
.64
.64
.72
.68
.62
.71
.70
.70
.65
.72
.69
.71
.70
.64
.64
.72
500.
458.
465.
476.
452.
477.
490.
458.
465.
476.
458.
477.
.68 471.
46,
44,
50.
52.
54,
55.
56,
57,
58.
58,
5«J.
58.
54.
44.
45,
45.
43.
46.
47.
48.
48,
50.
50.
51.
52.
47.
8.0
9.0
10.5
11.0
10.0
10.5
10.0
10.0
10.0
9.0
9.0
9.5
370
358
355
364
359
355
358
345
355
354
355
353
9.7
357.
43.
44.
43.
49.
50.
5«.
59.
59.
60.
59.
56.
52.
52.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAK LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST 05-3
STACK OUTLET *1 BATTERY
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1
£ VM
-J
TM
VMSTD
VLC
VMC
BHO
FMD
PC02
P02
PCO
PN2
MD
MWS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED TN
IMPINGERS AND SILICA GEL. ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL.. DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL.. DRY
PERCENT N2 BY VOL., DRY
MOLECULAR HT-DRY STACK GAS
MOLECULAR HT-STACK GAS
ENGLISH UNITS
12/12/81
135B
1558
120.0
12
.982
.402 IN
.84
.68 IN-H20
54.393 CU-FT
50.6 F
55.066 SCF
170.2
8.011 SCF
12.70
.873
3.70
11.80
.00
84.50
29.06
27.66
METRIC UNITS
12/12/81
1358
155B
120.0
12
.982
10.2 MM
.84
17.4 MM-H20
1.540 CU-M
10.3 C
1.559 SCM
170.2
.227 SCM
12.70
.873
3.70
11.80
.00
B4.50
29.06
27.66
-------
PB
PSI
PS
TS
VS
AS
OSSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLON RATE, DRV*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
29.78 IN-HG
-1.20 IN-H20
29.69 IN-HG
471. F
17.7 FPS
7505. 30-IN
1630772. SCFH
3327285. ACFH
99.6
.0000
.00000 GR/DSCF*
.00000 L8/HR
7S6.ai kM-HG
-30.4B CM-H20
754.17 *M-HG
204. C
5.a MPS
4.042 30-H
46292. SCfH
94219. ACfH
99.6
.0000
.0000 MG/DSCM
.000 KG/MR
EMISSION RATE
* 66 OEG f, 29.92 IN.HG.
00
-------
EXAMPLE PARTICIPATE CALCULATIONS TEST NO. 05-3
STACK OUTLET »1 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VM3TO « (17.647 * VM * Y * (PB + PM / 13.6)) / (TM » 460.)
17.647 • 50.393 • .482 * ( 29.78 » .683 / 13.6)
VMSTD * ---- • ------------------------------------------------ = 55.066 DSCF
( 51. * 060.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VHC * .04707 • VLC
VMC * .04707 * 170. s 8.01 SCF
PERCENT MOISTURE IN STACK GAS
BHO » (100. * VMC) / (VMSTD + VHC)
100. * 8.01
> BHO a —..——..———— — — s 12.70 PERCENT
I 55.066 «• 8.01
*»
-*.- ........
VO
MOLE FRACTION OF DRY STACK GAS
FMD « (100. - BHO) / 100.
100. - 12.7
— — ------ — a .873
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD • (PC02 • .44) 4 (PQ2 * .32) » (PN2 4 PCO) * .28
MD 3 ( 3.70*44/100) * (11.8*32/100) * ((83.5* .0) • 28/100 = 29.06
MOLECULAR HEIGHT OF STACK GAS
MHS s MD * (1. - (BNO/100)) + 18. * (BWO/10U)
MHS > 29.06* (1. -(12.70/100)) + 18. * (12.70/100) * 27.66
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SORT(VH * (TS * 460.))
VS 3 65.49 * CP * OELP / (SQRT(MhS * PS) * PNTS)
VS = 85.09 * .84 » 84.927 / (SORM 27.66 * 59.69) * 12. = 17.73 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS x VS • AS • 3600/144
OS * IT.73 * 7505. 3600/144 s 3327285. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTO * 17.647 • OS • PS • (1. - (BWO/100)) / (TS * 460.)
17.647 * 3327285. * 29.69 * (1. • (12.70/100))
OSSTO * ——————— -—.............................. s 1634772. SCFH
( 471. » 460.)
>
I PERCENT ISOKINETIC
*»
S ISO * (305.58*(TS«460.))*((0.002669*VLC)+(VM*Y*(PB*(PM/13.6))/(TM+460.)))/(TT*VS*PS*DN*DN)
(305.58M 471.«460.))*((0.002669* 170.)*( 54.393* ,982*( 29.78»( .683/13.6))/( 51.»460.)))
ISO x ..—..........................—[[[ 3 99.59 PERCENT
120. * 17.73 * 29.69 * .402 • .402
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN * 15.43 / VMSTO
CS s 0.001 * .0000 * 15.43 / 55.066 = .00000 GR/OSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR s CS * 03STD / (15.43 * 453.6)
-------
Run No. D5.3
3
Sample volume = 1.56m T 55.07 scf
Example calculations
CS (Part) =16.3/1.56 = 10.4 ma/m3
CS (Part) = 0.001 x 16.3x 15.43/55.07= 0.004 qr/dscf
CS (S02) =323.1 /1.56= 79.2ma/m3
= 79.2 x 24.06/64 =30 ppm
= 0.001 x123.6x 15.43££JE_eQJ135_ gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S0a=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
16.3
2.2
3.0
1.6
123.6
7.8
3 Concentration,
mg/m
10.4
1.4
1.9
1.0
79.2
5.0
gr/dscf
0.004
0.001
0.001
0.0004
0.035
0.002
ppm
30
1
A-451
-------
FIELD DAT*
UV
to
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET 01
SAMPLE TYPE PART
OPERATOR UAN FTIZGERALD
AMBIENT TEMP. (OEG.F) 36.
BAR. PRESS. (IN. HG) 29.78
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530335
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .84
THERM. NO. 133
LEAKAGE .019 CFM a 3.
METER CALIB. FACTOR 1.033
READ ft RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
BO.O
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
PI nrit i
I* UUL.TV f
1400
1410
1420
1430
1440
1050
1500
1510
1520
1530
1540
1550
1600
EVERY 10.0
GAS METER
READING
(CU.FT.)
412.927
417.135
421.690
426.235
430.800
435.175
439.825
444.395
449.040
453.645
458.030
462.430
467.086
MINUTES
VELOCITY
HEAD
(IN.H20)
.050
.055
.055
.055
.050
.057
.055
.055
.055
.050
.052
.057
CLEVELAND OHIO
BATTERY
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.62
.71
.70
.TO
.65
.72
.69
.71
.70
.64
.64
.72
H20)
ACTUAL
.62
.71
.70
.70
.65
.72
.69
.71
.70
.64
.64
.72
STACK
TEMP
(OEG.F)
500.
458.
465.
476.
452.
477.
490.
458.
465.
476.
458.
477.
DATE 12/12/81
RUN NUMBER ns-4
PROBE LENGTH ft TYPE 5 FOOT GLASS
NOZZLE : I.U. .401
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
KETEH BOX NUMBER FBO
METER HEAD OIFF. i.ee
PROBE HEATER SETTING 350.
HEATER BOX SETTING 350.
K FACTOR 11856.2
DRY GAS METER
TEMP
(OEG.F)
INLET OUTLET
51. 51.
52. 52.
57. 52.
61. 54.
64. 55.
66. 47.
66. 58.
68. 60.
70. 60.
70. 62.
70. 62.
69. 62.
PUMP
VACUUM
(IN.HG)
2.0
2.5
2.5
2.5
2.0
2.5
2.5
2.5
2.5
2.0
2.0
2.5
SAMPLE
BOX TEMP
(OEG.F)
352.
362.
347.
344.
367.
345.
348.
344.
350.
352.
350.
352.
IMPIN6ER
TEMP
(DEG.F)
42.
43.
45.
48.
52.
54.
58.
59.
59.
62.
57.
49.
TOTALS
AVERAGE
120.0
54.159
.68
.68 471.
64.
57.
2.3 351.
52.
-------
PARTICIPATE FIELD DATA * RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FTIZGERALD
TtST D5-4
STACK OUTLET 01 BATTERY
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
12/12/81
1400
1600
120
12
1
.0
.033
.401 IN
.84
.68 IN-H20
METRIC UNITS
12/12/61
1400
1600
120
12
1
10
17
.0
.033
.2
.84
.4
PM
PM-I
I/I—
OJ
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VHC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BNO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
PD2 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR NT-DRY STACK GAS
MHS MOLECULAR HT-STACK GAS
54.159 CU-FT
60.5 F
56.586 SCF
182.8
8.604 SCF
1.534 CU-M
15.8 C
1.602 SCM
182.8
.244 SCM
13.20
.868
3.70
11.80
.00
84.50
29.06
27.60
13.20
.868
3.70
11.80
.00
84.50
29.06
27.60
-------
PB
PS
TS
VS
AS
OSSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE* DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
29.78 IN-HG
-1.20 IN-H20
29.69 IN-HG
071. F
17.6 FPS
7505. SQ-IN
1627070. SCFH
3330605. ACFH
103.3
.0000
.00000 GR/DSCF*
.00000 LB/HR
756.41 *M-HG
•30.48 *M-H20
754.17 *M-HG
244. C
5.4 VPS
4.842 SO-M
46074. 3CHH
94313. ACMH
103.3
.0000
.0000 MG/D3CM
.000 KG/MR
EMISSION RATE
* 68 OEG F, 29.93 IN.HG.
*"
en
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. D5-4
STACK OUTLET *1 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD « 117.647 * VM • Y * (PB * PM / 13.6)) / (TM * 460.)
17.647 • 54.154 • 1.033 * ( 29. 7B * .683 / 13.6)
VMSTD * — -------------------------------------------------- a 56.586 DSCF
I 60. » 460.)
VOLUME OF WATER VAPOR AT STANDARD CONDITIONS
VMC * .04707 * VLC
VHC • .04707 * 183. = 8.60 SCF
PERCENT MOISTURE IN STACK GAS
8*0 * (100. * VMC) / (VMSTD + VHC)
> 100. * 8.60
I BNO * ------------------------- - = 13.20 PERCENT
^ 56.586 4 8.60
Ul
MOLE FRACTION OF DRY STACK GAS
FMD * (100. - BMO) / 100.
100. - 13.2
FMD « —————————— s .868
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO « (PC02 * .44) * (PQ2 • .32) * (PN2 * PCO) • .28
MO = ( 3.70*44/100) » (11.8*32/100) * ((84.5* .0) • 28/100 = 29.06
MOLECULAR HEIGHT OF STACK GAS
MMS * MD * (1. - (BMO/100)) «• 18. * (RwO/100)
MMS » 29.06* (1. -(13.20/100)) + 18. * (13.20/100) s 27.60
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP = SUM. Of THE SORUVH * (TS + 460.))
VS « 85.49 * CP • OELP / (SQRT(M*S * PS) * PNTS)
VS = 85.49 * .84 « 84.927 / (SGRT( 27.60 * 29.69) * 12. s 17.75 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
03 3 VS * AS * 3600/144
OS = 17.75 * 7505. 3600/144 s 3330605. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTD = 17.647 * OS * PS * (1. - (BWO/100)) / (TS * 460.)
17.647 * 3330605. * 29.69 * (1. - (13.20/100))
OSSTD e ...................—.—.. ...—. .. . = 1627070. SCFH
( 471. * 460.)
> PERCENT ISOKINETIC
£; ISO = (305.5B*(TS»460.))*((0.002669*VLC)+(VM*Y*(PB*(PM/13.6))/(TM*460.)))/(TT*VS*PS*DN*ON)
a\
(305.58*( 471.«460.))*( (0.002669* 183.)»( 54.159*1.033*( 29.78+( .683/13.6))/( 60.«460.)))
ISO « . ....... a 103.34 PERCENT
120. * 17.75 * 29.69 * .401 * .401
PARTICIPATE LOADING -- EPA METHOD 5 (AT STANDARD CONDITIONS)
CS 3 0.001 * MN * 15.43 / VMSTD
CS s 0.001 * .0000 * 15.43 / 56.586 = .00000 GR/OSCF
PARTICULATE LB3/HR — EPA METHOD 5
PMR s CS * OSSTD / (15.43 * «53.6)
PMR * .00000 * 1627070. / (15.43 * 453.6) = .00000
-------
Run No. D5.4
3
Sample volume = 1.60m T 56.59 scf
Example calculations
CS (Part) =19.1 /1.60= 11.9 mq/m3
CS (Part) = 0.001 x19.1 x 15.43/56.59 = 0.005 gr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ = gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
19.1
0.6
0.8
3.8
158.1
4.0
572
o Concentration,
mg/m
11.9
0.4
0.5
2.4
98.8
2.5
357
gr/dscf
0.005
0.0002
0.0002
0.001
0.043
0.001
0.156
ppm
IPA contaminated
A-457
-------
FIELD DATA
*>
U1
00
PLANT REPUBLIC STEEL
SAMPLING LOCATION CUKE STACK
SAMPLE TYPE M5-250
OPERATOR DU
AMBIENT TEMP. (DEG.F) 40.
BAR. PRESS. (IN. HG) 29.78
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER I b)
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .83
THERM. NO.
LEAKAGE .000 CFM 9 2.
METER CALI8. FACTOR .992
READ ft RECORD DATA
TRAVERSE
POINT
NO.
IN1T
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30. V
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(20-HR
f i fir* K i
l»LU(* K t
1358
1408
1418
1428
1438
1448
1458
1508
1518
1528
153B
1548
1558
EVERY 10.0
GAS METER
READING
(CU.FT.)
133.219
138.090
142.910
147.760
152.610
157.480
162.360
167.270
172.140
177.040
182.000
186.900
191.818
MINUTES
VELOCITY
HEAD
(IN.H20)
.052
.052
.052
.052
.052
.052
.052
.052
.052
.052
.052
.052
CLEVELAND
5 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.76
.76
.76
.76
.76
.76
.76
.76
.76
.76
.76
.76
H20)
ACTUAL
.76
.76
.76
.76
.76
.76
.76
.76
.76
.76
.76
.76
STACK
TEMP
(DEG.F)
500.
458.
465.
476.
452.
477.
490.
458.
465.
476.
458.
477.
DATE 12/12/41
RUN NUKBER 05-5
PROBE LENGTH ft TYPE 5' GLASS
N02/LE : I.D. .434
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
METER BOX NUMBER FBI
METER HEAD OIFF. 1.87
C FACTOR .71
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .13
DhY GAS fETER
TEMP
(DEG.F)
ULET OUTLET
45. 42.
48. 42.
53. 42.
57. 43.
60. 44.
61. 46.
63. 46.
65. 48.
65. 49.
66. 50.
67. SO.
.67. 51.
PUMP
VACUUM
(IN.HG)
.5
.5
.5
.5
.5
.5
.5
.5
1.0
1.0
1.0
1.0
SAMPLE
BOX TEMP
(OEG.F)
237.
21«.
282.
252.
275.
230.
271.
218.
252.
268.
220.
283.
IMPINGER
TEMP
(DEG.F)
44.
44.
46.
46.
47.
48.
48.
48.
48.
50.
50.
51.
TOTALS
AVERAGE
120.0
58.599
.76
.76
471.
60,
46.
.7 251.
48,
-------
PARTICIPATE FIELD DATA & RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO
TEST D5-5
COKE STACK
Ul
TEST
TB
TF
TT
NP
Y
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
ENGLISH UNITS
12/12/81
1358
1558
120.0
12
.992
.434 IN
.63
.76 1N-H20
METRIC UMTS
12/12/81
1358
1558
120.0
12
.992
11.0
.83
19.3
KM
PM-I
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGEUS AND SILICA GEL."L.
VHC VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
BHO PERCENT MOISTURE BY VOLUME
FMO MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL.. DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR HT-ORY STACK GAS
MHS MOLECULAR HT-STACK GAS
58.599 CU-FT
52.9 F
59.671 SCF
177.8
8.369 SCF
1.659 CU-M
11.6 C
1.690 SCP
177.8
.237 SCM
12.30
.877
3.70
11.80
.00
84.50
29.06
27.70
12.30
.877
3.70
11.80
.00
84.50
29.06
27.70
-------
PB
PSI
PS
TS
VS
AS
QSSTD
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES. A3S.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE* DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
EMISSION RATE
* 68 DEC F, 29.92 IN.HG.
39.78 IN-HG
-1.20 1M-H20
29.69 IN-MG
471. F
17.2 FPS
7466. SO-IN
1585882. SCFH
3213030. ACFH
95.0
.0000
.00000 GR/DSCF*
.00000 LB/HR
756.41 fM-HG
-30.48 MM-H20
754.17 MM-HG
240. C
5.2 fPS
4.817 SO-M
44907. SCMH
90983. ACMH
95.0
.0000
.0000 MG/OSCM
.000 KG/HR
it^
CT>
O
-------
EXAMPLE PARTICULATE CALCULATIONS TfcST NO. D5-5
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO » (17.607 * VM • Y * (PB * PM / 13.6)) / (TM * 060.)
17.607 • 58.599 * .992 * ( 29.78 * .760 / 13.6)
VMSTD * ————————.. — ....... ..—... ... - 59.671 OSCF
( 53. «• 060.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VHC = .00707 • VLC
VHC * .00707 * 178. = B.37 SCF
PERCENT MOISTURE IN STACK GAS
BHO s (100. • VHC) / (VMSTD * VHC)
100. * 8.37
BHO = — • * 12.30 PERCENT
59.671 * 8.37
MOLE FRACTION OF DRY STACK GAS
FMD = (100. > BHO) / 100.
100. - 12.3
FMD * —————......... - .877
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD * (PC02 * .00) * (P02 * .32) * (PN2 «• PCCI) * .28
MO = ( 3.70*00/100) * (11.8*32/100) * ((80.5* .0) * 28/100 = 29.06
MOLECULAR HEIGHT OF STACK GAS
MHS = MD * (1. - (BHO/100)) * 18. * (BWO/100)
MHS = 29.06* (1. -(12.30/100)) * 18. * (12.30/100) = 27.70
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP s SUM. OF THE SORT(VH * (TS + 460.))
VS » 85.19 * CP • DELP / (SQRT(MhS * PS) * PNTS)
VS = 85.09 * .83 * 83.192 / (SOWT( 27.70 • 29.69) * 12. = 17.21 FPS
STACK GAS VOLUMETRIC FLOH AT STACK CONDITIONS
OS = VS * AS • 3600/104
OS s 17.21 * 7066. 3600/100 z 3213030. ACFH
STACK GAS VOLUMETRIC FLO* AT STANDARD CONDITIONS
OSSTO z 17.607 * OS * PS * Cl. - (BwO/100)) / (TS * 060.)
17.647 * 3213030. * 29.69 • (1. - (12.30/100))
OSSTO a = 1585882. SCFH
( 071. «• 460.)
jp PERCENT ISOKINETIC
•**• ISO = (305.58*(TS*060.))*((0.002fc69*VLC)*(VI"'*Y*(PB*(PM/13.6) )/(TM4060.)))/(TT*VS«PS*DN*ON)
o\
M (305.58*C 071.+060.))*((0.002669* 178.)*( 58.599* ,992*( 29.78M .760/13.6))/( 53.»060.)))
ISO s . — = 94.96 PERCENT
120. * 17.21 * 29.69 * .030 * .030
PARTICIPATE LOADING -- EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 * MN • 15.03 / VMSTD
CS - 0.001 * .0000 * 15.03 / 59.671 = .00000 GR/DSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR = CS * OSSTD / (15.03 * 053.6)
PMR » .00000 * 1585882. / (15.03 * 053.6) = .00000
-------
Run No. D5.5
3
Sample volume =1.69 m . 59.67 scf
Example calculations
CS (Part) =15.9/1.69= 9.4 ma/rn3
CS (Part) = 0.001 x 15.9x 15.43/59.67= 0.004qr/dscf
CS (S02) = /.
.mg/nT
x 24.06/_
.ppm
= 0.001 x.
.x 15.43/.
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04I
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
15.9
6.9
5.3
4.5
4.5
2.4
0.0
0.0
0.0
15.6
1.4
3.6
, Concentration,
mg/m
9.4
4.1
3.1
2.7
2.7
1.4
0.0
0.0
0.0
9.2
0.83
2.1
gr/dscf
0.004
0.002
0.001
0.001
0.001
0.001
0.000
0.000
0.000
0.004
0.0004
0.0009
ppm
A-463
-------
FIELD DAT*
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEC.F)
BAR.PRESS. UN.MG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEfcL CLEVELAND
COKE STACK
M8-600
DO
40.
39.78
-1.20
97.50
.83
,00
.008 CFM 9 I 1.5 IN.HG
.967
DATE 12/12/81
HUN NUMBER 05-6
PROBE LENGTH ft TYPE a* GLASS
NUZZLE : I.D. .379
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
PETER BOX NUMBER FBb
METER HEAD OIFF. 1.51
C FACTOR .90
PROBE HEATER SETTING 600.
HEATER BOX SETTING 600.
REFERENCE PRESS. DIFF. .lb
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE
POINT TIME
NO. (MIN.)
INIT 0
10.0
> 20.0
^ 30.0
40.0
*» 50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
n nrv i
UI.UI* A J
1359
1409
1419
1429
1439
1449
1459
1509
1519
1529
1539
1549
1559
GAS METER VELOCITY ORIFICE PRESSURE STACK
READING HEAD DIFFERENTIAL TE*P
(CU.FT.) (IN.H20) (IN.H20) (DEG.F)
DESIRED
881.913
886.620
891.270
895.980
900.700
905.420
910.120
914.850
919.580
924.320
929.120
933.880
938.607
.052
.052
.052
.052
.052
.052
.052
.052
.052
.052
.052
.052
.55
.55
.55
.55
.55
.55
.55
.55
.55
.55
.55
.55
ACTUAL
.55
.55
.55
.55
.55
.55
.55
.55
.55
.55
.55
.55
DRY GAS METER PUMP SAMPLE
TEMP VACUUM BOX TEMP
(DEG.F) (IN.HG) (DEG.F)
IMPJNGER
TEMP
(OEG.F)
INLET OUTLET
500.
458.
465.
476.
452.
477.
490.
458.
465.
476.
458.
477.
39.
40.
44.
47.
49.
50.
51.
52.
52.
52.
52.
53.
41.
41.
41.
41.
42.
42.
42.
43.
43.
44.
44.
44.
4.3
4.8
7.2
7 .*>
7.5
8.8
10.0
10.3
10.8
11.2
11.0
11.2
555.
598.
620.
620.
623.
608.
607.
605.
600.
594.
587.
586.
42.
42.
44.
46.
4b.
47.
47.
48.
48.
49.
49.
49.
TOTALS
AVERAGE
120.0
56.694
.55
.55
471,
48,
42.
6.7
600.
46.
-------
PARTICULATE FIELD 0»T» ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO
TEST 05-6
COKE STACK
Xn
ENGLISH UNITS METRIC UNITS
TEST
TB
TF
TT
NP
V
DN
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MlN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
12/12/81 12/12/81
1359 1359
1559 1559
120.0 120.0
12 12
.967 .967
.379 IN 9.6
.A3 .83
.55 IN-H20 14.0
PM
KM-I
DROP
VM VOLUME OF DRV GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VWC VOLUME OF MATER VAPOR
AT STANDARD CONDITIONS*
8MO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRV GAS
PC02 PERCENT C02 BY VOL.* DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., ORY
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR HT-DRY STACK GAS
MMS MOLECULAR MT-STACK GAS
56.694 CU-FT
45.4 F
57.087 SCF
144.1
6.783 SCF
10.62
.894
3.70
11 .80
.00
84.50
29.06
27.89
1.605 CU-M
7.4 C
1.617 SCP
144.1
.192 SCf
10.62
.894
3.70
11.80
.00
84.50
29.06
27.B9
-------
PB
PSI
PS
T3
VS
AS
OSSTO
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES Of STACK GAS
STACK PRFSr ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATEf DRY*
ACTUAL STACK FLO* RATE
PERCENT ISOKINETIC
MG. EPA 5
29.78 IN-HG
-1.50 IN-H20
a9.69 IN-HG
171. F
17.? FPS
7066. SQ-IN
161087?. SCFH
3202302. ACFH
117.3
.0000
.00000 GR/DSCF*
.00000 LB/HR
756.
-------
EXAMPLE PARTICULATE CALCULATIONS ttST NO. D5-6
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 • VM • Y * (PB » PM / 13.6)) / (TM + 460.)
17.647 * 56.694 • .967 * ( 29.78 «• .550 / 13.6)
VMSTD » ——--— — — = 57.087 DSCF
t 45. » 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC a .04707 • VIC
VNC a .04707 * 144. = 6.78 SCF
PERCENT MOISTURE IN STACK GAS
BMO a (100. • VNC) / (VMSTD * VWC)
100. * 6.78
•.,, BMO a — ———— — — ... = 10.62 PERCENT
I 57.087 * 6,78
4*.
cn
«j
MOLE FRACTION OF DRY STACK GAS
FMD a (100. - BMO) / 100.
100. • 10.6
FMD s ——............. ... s .894
100.
AVERAGE MOLECULAR WEIGHT OF DRY STACK GAS
MD a (PC02 • .44) * (P02 * .38) * (PN2 * PCO) * .28
MD * ( 3.70*44/100) + (11.8*32/100) * 1(84.5* .0) * 28/100 = 29.06
MOLECULAR HEIGHT OF STACK GAS
MhS a MD * (1. - (BMO/10U)) » 18. * (BMO/1UO)
MWS a 29.06* (1. -(10.62/100)) » 18. * (10.62/100) a 27.89
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SQRHVH * ITS * 060.))
VS * 85.49 * CP » DELP / (SQRUMHS * PS) • PNTS)
VS = 8S.49 * .83 * 03.498 / (SQRT( 27.fl9 * 29.69) * 12. : 17.16 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
US * VS • A3 * 3600/144
OS = IT.16 * 7466. 3600/144 = 3202302. ACFH
STACK GAS VOLUMETRIC FLOH AT STANDARD CONDITIONS
OSSTD = 17.647 * OS * PS * (1. - (BMO/100)) / (TS * 460.)
17.647 • 3202302. * 29.69 • (1. - (10.62/100))
OSSTD = —— —— .....— ...... . — . = 1610872. SCFH
( 471. » 460.)
PERCENT I30KINETIC
>
| ISO * (305.5B«(T3«460.))<»((0.002669*VLC)»(VM*Y«(PB+(PM/13.6))/(TM*460.)))/(TT«VS»PS«DN«DN)
.U
J? (305.5SM 471.+460.))*((0.002669* 144.)+( 56.694* ,967«( 29.78«( .550/13.6))/( 05.+460.)))
ISO = — " • = 117.28 PERCENT
120. * 17.16 • 29.69 • .379 * .379'
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 • MN * 15.43 / VMSTD
CS = 0.001 • .0000 * 15.43 / 57.087 = .00000 GR/DSCF
PAHTICULATE LBS/HR — EPA METHOD 5
PMR = CS * QSSTO / (15.43 * 453.6)
PHR « .00000 * 1610872. / (15.43 * 453.6) = .00000
-------
Run No. D5.6
Sample volume =1.62 m3r 57.09 scf
Example calculations
CS (Part) =12.9/1.62=8.0 mq/m3
CS (Part) = 0.001 x 12.9X 15.43/57.09 = 0.003 qr/dscf
3
CS (S02) =129.0/1.62= 79.6mq/nr
= 79.6 x 24.06/64 =30 ppm
= 0.001 x!29.0x 15.43/57.09
0.035 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sulfates
As H2S04
As H2S04.2H20
Water soluble sulfates
As S04S
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
12.9
0.3
0.4
1.4
129.0
8.2
3 Concentration,
mg/m
8.0
0.2
0.2
0.9
79.6
5.1
gr/dscf
0.0003
0.0001
0.0001
0.0003
0.035
0.002
ppm
30
1
A-469
-------
FIELD DATA
PLANT
SAMPLING LOCATION
SAMPLE TYPE
OPERATOR
AMBIENT TEMP.(DEC.F)
BAR.PRESS.(IN.HG)
STATIC PRESS.(IN.H20)
FILTER NUMBER(S)
STACK INSIDE DIM.(IN)
PITOT TUBE COEFF.
THERM. NO.
LEAKAGE
METER CALIB. FACTOR
REPUBLIC STEtL CLEVELAND
COKE OUTLET
PART/H2S04/S02
ARMSTRONG
38.
29.79
-1.20
97.75
.84
.000 CFM a
1.003
.00
6.0 IN.HG
READ ft RECORD DATA EVERY 10.0 MINUTES
DATE
RUN NUMBER
PROBE LENGTH & TYPE
NOZZLE : I.U.
ASSUMED MOISTURE
SAMPLE BOX NUMBER
METER BOX NUMBER
METER HEAD OIFF.
C FACTOR
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE PRESS. DIFF.
12/13/81
Ub-1
5 FT GLASS
13.7
0
FB2
1.76
.78
250.
250.
.15
TRAVERSE
POINT
NO.
SAMPLE
TIME
(MIN.)
CLOCK
TIME
(24-HR
LLUUK >
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
ORIFICE PRESSURE
DIFFERENTIAL
(IN.H20)
DESIRED ACTUAL
STACK
TEMP
(DEG.F)
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPINGER
TEMP
(DEG.F)
INIT
TOTALS
AVERAGE
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
120.0
945
955
1005
1015
1025
1035
1045
1055
1105
1115
1125
1135
1145
531,
535,
539,
544,
548.
552.
557.
561.
565.
570,
574.
578,
583.
010
645
880
220
405
640
145
000
770
135
400
920
020
.050
.046
.048
.045
.046
.050
.047
.045
.047
.045
.050
.045
52.010
.62
.56
.59
.55
.56
.62
.58
.55
.58
.55
.62
.55
.58
.62
.56
.59
.55
.56
.62
.58
.55
.58
.55
.62
.55
.58
ass.
463,
465.
443.
456.
463.
447.
460.
460.
440.
448.
461.
455.
35.
38.
41.
44.
44.
44,
45.
45,
46.
46.
46,
06.
43.
35.
35.
35.
35.
36.
36.
37.
38.
37.
38.
40.
40.
37.
1.5
2.5
2.5
3.0
4.2
4.8
5.1
5.1
5.0
5.0
5.5
5.5
259.
262.
290.
261.
284.
280.
265.
271.
263.
265.
236.
302.
4.1 270.
41,
39.
40.
40.
40.
45.
47,
45.
45.
46.
52.
54.
45.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND ARMSTRONG
TEST D6-1
COKE OUTLET
TEST DATE
TB
TF
TT
NP
V
DN
CP
PM
i. VM
-J
TM
VMSTD
VLC
VHC
BNO
FMO
PC02
P02
PCO
PN2
MO
MHS
TIME-START
TIME-FINISH
NET TIME OF TEST. MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR WT-STACK GAS
ENGLISH UNITS
12/13/81
945
1105
120.0
12
1.003
.404 IN
.64
.58 IN-H20
52.010 CU-FT
40.1 F
50.917 SCF
153.0
7.202 SCF
11.59
.884
5.10
11.00
.00
83.90
29.26
27.95
METRIC UNITS
12/13/81
945
1145
120.0
12
1.003
10.3
.84
14.7
1.473
4.5
1.555
153.0
.204
11.59
.884
5.10
11.00
.00
83.90
29.26
27.95
KM
PM-H20
CU-M
C
SCM
SCM
-------
PH
PSI
PS
TS
VS
AS
OSSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES. ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE* DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
29.79 IN-HG
-1.20 IN-H2U
39.70 IN-HG
455. F
16.3 FPS
7505. SO-IN
1552508. SCFH
3065694. ACFH
103.5
.0000
.00000 GR/DSCF*
.00000 LB/HR
756.67 *M-HG
-30.48 PM-H20
754.42 CM-HG
235. C
5.0 *P3
4.642 SO-M
43962. SCMH
66617. ACPH
103.5
.0000
.0000 MG/DSCM
.000 KG/HR
EMISSION RATE
* 68 DEC f, 29.92 IN.HG.
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 06-1
COKE OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VHSTD = (17.647 • VM * Y * (PB t PM / 13.6)) / (TH * 460.)
17.6*7 • 52.010 • 1.003 • ( 29.79 «• .577 / 13.6)
VMSTO = —. ——......... ... ..... ._ . = 50.917 OSCF
( 40. + 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC = .04707 * VLC
VMC * .04707 * 153. = 7.20 SCF
PERCENT MOISTURE IN STACK GAS
BMO • (100. * VMC) / (VMSTD * VMC)
> 100. • 7.20
I BMO * ——-——-—— ....... = 11.59 PERCENT
^ 54.917 * 7.20
oo
MOLE FRACTION OF DRY STACK GAS
FMO s (100. > BMO) / 100.
100. > 11.6
FMO = -.———— ........ , .884
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MO r (PC02 * .44) * (P02 * .32) * (PN2 * PCO) * .28
MD = ( 5.10*44/100) * (11.0*32/100) » ((83.9* .0) * 28/100 a 29.26
MOLECULAR HEIGHT OF STACK GAS
MMS = MD • (1. - (BWO/100)) » 18. * (BWO/100)
MhS = 29.26* (1. -(11.59/100)) +18. * (11.59/100) z 27.95
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SORUVH * US » 460.))
VS » 85.49 • CP * OELP / (SQRMMWS * PS) * PNTS)
VS » 85.49 * .84 • 78.681 / (SORT! 27.95 • 29.70) * 12. = 16.34 FPS
STACK GAS VOLUMETRIC FLO" AT STACK CONDITIONS
OS = VS * A3 * 3600/144
OS e 10.34 * 7505. 3600/144 = 3065894. ACFH
STACK GAS VOLUMETRIC FLO* AT STANDARD CONDITIONS
OSSTD a IT.647 * (IS • PS * (1. - (BWO/100)) / (TS « 460.)
17.647 • 3065894. • 29.70 • (1. • (11.59/100))
OSSTD * = 1552508. SCFH
( 455. » 460.)
PERCENT ISOKINETIC
ISO = (305.58*(TS*460.))*({0.002669«VLC)+(VM«YMPB*(PM/13.6))/(TM*460.)))/(TT«VS«PS«DN*ON)
(305.58»( 455.«460.))*((0.002669* 153.)*( 52.010*1.003*( 29.79*( .577/13.6))/1 4U. + 460.)))
ISO s . s 103.55 PERCENT
120. * 16.34 * 29.70 * .404 • .404
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS s 0.001 * MN * 15.43 / VMSTO
CS s 0.001 • .0000 * 15.43 / 54.917 = .00000 GR/DSCF
PARTICIPATE LBS/HR -- EPA METHOD 5
PMR = CS * OSSTD / (15.43 * 453.6)
PUR * .00000 * 1552508. / (15.43 * 453.6) = .00000
-------
Run No. D6.1
*3
Sample volume =JL_56_m T 54.92 scf
Example calculations
CS (Part) =12.2 /1.56= 7.8 mq/m3
CS (Part) = 0.001 x12.2 x 15.43/54.92= 0.003 qr/dscf
CS (S02) =118.3/1.56= 75.8mg/m3
= 75.8 x 24.06/64 = 28 ppm
= 0.001 x118.3 x 15.4364.92 = 0.033 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
12.2
0.0
0.0
0.0
118.3
13.2
2 Concentration,
mg/m
7.8
0.0
0.0
0.0
75.8
8.5
gr/dscf
0.003
0.000
0.000
0.000
0.033
0.004
ppm
28
2
A-47.5
-------
FIELD OAT*
I
CTt
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE OUTLET
SAMPLE TYPE PART
OPERATOR ARMSTRONG
AMBIENT TEMP. (DEG.F) 32.
BAR. PRESS. (IN. HG) 29.79
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBEM(S)
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .84
THERM. NO.
LEAKAGE .002 CFM 3 4.
METER CALIB. FACTOR 1.004
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE SAMPLE CLOCK GAS METER VELOCITY
POINT
NO.
INIT
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
TIME
(24-HR
pi r\ p w \
LLUUK I
947
957
1007
1017
1027
1037
1047
1057
1107
1117
1127
1137
1147
READING
(CU.FT.)
655.605
660.100
664.425
668.850
673.140
677.450
681.980
686.350
690.700
695.000
699.430
704.020
708.370
HEAD
(IN.H20)
.050
.006
.008
.005
.046
.050
.047
.045
.047
.045
.050
.045
CLEVELAND
0 IN.HG
ORIFICE PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.62
.56
.59
.55
.56
.62
.58
.55
.58
.55
.62
.55
H20)
ACTUAL
.62
.56
.59
.55
.56
.62
.58
.55
.58
.55
.62
.55
STACK
TEMP
(DEG.F)
455.
463.
465.
403.
456.
463.
447.
460.
460.
060.
008.
461.
DATE 12/13/81
RUN NUMBER 06-2
PROBE LENGTH ft TYPE o FT GLASS
NOZZLE : I.U. .400
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER 0
METER BOX NUMBER FB7
METER HEAD OIFF. I.TI
C FACTOR .76
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. D1FF. .15
DRY GAS METER PUMP SAMPLE IMP1NGER
TEMP VACUUM
(DEC
INLET
40.
42.
47.
51.
53.
55.
56.
57.
58.
58.
58.
58.
.F) (IN.HG)
OUTLET
38.
38.
38.
40.
40.
42.
43.
44.
44.
46.
46.
47.
.2
.5
.5
.5
.5
.5
.5
.5
.5
.5
.5
.5
BOX TEMP
(DEG.F)
270.
267.
260.
240.
258.
244.
232.
246.
245.
224.
22fc.
260.
TEMP
(DEG.F)
41.
37.
40.
41.
42.
43.
43.
44.
50.
51.
49.
55.
TOTALS
AVERAGE
120.0
52.765
.58
.58
457.
53.
42.
1.5 248.
45.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND ARMSTRONG
TEST 06-2
COKE OUTLET
ENGLISH UNITS
TEST
TB
TF
TT
NP
Y
ON
CP
PM
DATE
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
12/13/81
947
1147
120
12
1
.0
.004
.400 IN
.84
.58 IN-H20
METRIC UNITS
12/13/B1
947
1147
120
12
1
10
14
.0
.004
.2
.84
.7
VM
PM-I
DROP
VM VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
TM AVERAGE GAS METER TEMP
VMSTD VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML,
VMC VOLUME OF WATER VAPOR
AT STANDARD CONDITIONS*
BHO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRY
PN2 PERCENT N2 BY VOL., DRY
MO MOLECULAR HT-DRY STACK GAS
MhS MOLECULAR NT-STACK GAS
52.765 CU-FT
1.494 CU-M
47.5 F
54.959 SCF
171.0
8.049 SCF
12.77
.H72
5.10
11.00
.00
83.90
29.26
27.82
8
1
171
12
5
11
83
29
27
.6 C
.556 SCM
.0
.228 SCM
.77
.872
.10
.00
.00
.90
.26
.82
-------
PB
PSI
PS
T8
VS
AS
OS3TO
OS
ISO
MN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLON RATE* DRV*
ACTUAL STACK FLON RATE
PERCENT ISOKINETIC
MG. EPA 5
29.7<» IN-HG
-1.20 IN-H20
29.70 IN-HG
457. F
16.a FPS
7505. SO-IN
1534002. SCFH
3075956. ACFH
107.0
.0000
.00000 GR/DSCF*
.00000 LB/HR
EMISSION RATE
* 68 DEC F, 29.92 IN.H6.
756.67 KM-HG
-30.48 PM-H20
754.03 f»M-MG
236. C
5.0 fPS
4.842 SO-M
43438. SCHH
87102. ACMH
107.0
.0000
.0000 MG/OSCM
.000 KG/HR
00
-------
EXAMPLE PART1CULATE CALCULATIONS TEST NO. D6-2
COKE OUTLET
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD s (17.647 * VM * Y • (PB * PM / 13.6)) / (TM » 060.)
17.607 * 52.765 * 1.000 * ( 29.79 «• .577 / 13.6)
VMSTD = ——— — —— ——................. ... ... = 54.959 DSCF
( 07. » 060.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VMC « .00707 • VLC
VMC * .00707 * 171. s 8.05 SCF
PERCENT MOISTURE IN STACK GAS
BMO 8 (100. « VMC) / (VMSTD * VMC)
100. * 8.05
BMO » = 12.77 PERCENT
50.959 «• 8.05
MOLE FRACTION OF DRY STACK GAS
FMD = (100. - BMO) / 100.
100. - 12.8
FMD s s .872
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD s (PC02 • .00) * (P02 * .32) * (PN2 * PCO) * .28
MD * ( 5.10*00/100) * (11.0*32/100) * ((83.9* .0) • 28/100 = 29.26
MOLECULAR HEIGHT OF STACK GAS
MMS ' MD * (1. - (BMO/100)) «• IB. * (8*0/100)
MMS * 29.26* (1. -(12.77/100)) + 18. * (12.77/100) s 27.82
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE SORT(VH * (TS + 460.))
VS s 85.49 • CP * DEUP / ISQRT(MWS » PS) • PNTS)
V3 = 85.49 * .84 • 78.751 / (SGRTl 27.fl? * 89.70) • 12. = 16.40 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS * VS * AS * 3600/144
OS * 16.40 • 7505. 3600/144 = 3075958. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD = 17.647 * OS * PS * (1. • (BNO/100)) / (TS * 460.)
17.647 • 3075958. • 89.70 « (I. - (12.77/100))
OSSTO f s 1534002. SCFH
( 457. * 460.)
> PERCENT ISOKINETIC
I
TO ISO * (305.58*(T3*460.))*((0.002669*VLC)*(VM*Y*(PB*(PM/13.6))/(TM+460.)))/ITT*VS*PS*DN*ON)
O
(305.5BM 457.4460.))*((0.002669* 171.)*( 58.765*1.004*( 89.79*( .577/13.6))/( 47.»460.)))
ISO = —————————.-.. —...................—..... ................................ c 106.99 PERCENT
120. * 16.40 * 29.70 * .400 * .400
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS s 0.001 * MN * 15.43 / VMSTD
CS r 0.001 * .0000 * 15.43 / 54.959 = .00000 GR/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR > CS * OSSTD / (15.43 • 453.6)
PMR s .00000 * 1534002. / (15.43 * 453.6) = .00000
-------
Run No. D6.2
Sample volume = 1.56 m f 54.96 scf
Example calculations
CS (Part) =21.1/1.56= 13.5 mg/m3
CS (Part) = 0.001 x 21.1 x 15.43/54.96 = 0.006 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x x 15.43/ =
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
21.1
5.4
0.0
0.0
0.0
55.2
2.4
403
~ Concentration,
mg/m
13.5
3.5
0.0
0.0
0.0
35.4
1.5
258
gr/dscf
0.006
0.001
0.000
0.000
0.000
0.015
0.0007
0.113
Ppm
IPA contaminated
A-481
-------
FIELD DATA
00
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET 01
SAMPLE TYPE PART/H2S04/S02
OPERATOR HAN FITZGERALD
AMBIENT TEMP. (DEC. F) 32.
BAR. PRESS. (IN.HG) 29.79
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530059
STACK INSIDE DIM. (IN) 97.75 .00
PITOT TUBE COEFF. .60
THERM. NO. 133
LEAKAGE .002 CFM a) 5.
METER CALIB. FACTOR .982
READ ft RECORD DATA
TRAVERSE
POINT
NO.
IN1T
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
00.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
945
955
1005
1015
1025
1035
1045
1055
1105
1115
1125
1135
1145
EVERY 10.0
GAS METER
READING
(CU.FT.)
911.166
915.480
919.560
923.675
927.765
931.700
936.000
900.205
900.290
908.480
952.700
957.105
961.260
MINUTES
VELOCITY
HEAD
(IN.H20)
.050
.046
.048
.005
.006
.050
.047
.045
.007
.045
.050
.005
CLEVELAND OHIO
BATTERY
0 IN.HG
ORIFICE
PRESSURE
STACK
DIFFERENTIAL TE"P
(IN.
DESIRED
.60
.58
.60
.58
.58
.63
.60
.57
.59
.58
.60
.57
H20)
ACTUAL
.60
.58
.60
.58
.58
.63
.60
.57
.59
.58
.60
.57
(DEG.F)
DATE 12/13/81
RUN NUMBER 06-3
PROBE LENGTH ft TTf-E a FOOT GLASS
NOZZLE : l.D. .400
ASSUMED MOISTURE 13.2
SACPLE BOX NUMBER
PETER BOX NUMBER FB8
METFR HEAD OIFF. 1.91
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
K FACTOR 11628.3
DRY GAS
TEMP
(DEG.
METER
F)
PUMP
VACUUM
(IN.HG)
SAMPLE
BOX TEMP
(DEG.F)
IMPINGER
TEMP
(DEG.F)
INLET OUTLET
455.
063.
065.
443.
455.
463.
047.
060.
060.
000.
446.
461 .
34.
36.
43.
48.
50.
52.
54.
54.
55.
55.
56.
56.
32.
33.
35.
37.
40.
42.
04.
45.
06.
07.
48.
48.
2.5
2.5
2.5
2.5
3.0
4.5
4.5
4.5
5.0
5.0
5.0
5.0
407.
401.
401.
399.
404.
407.
406.
402.
397.
391.
387.
387.
40.
44.
42.
42.
43.
41.
49.
49.
57.
60.
60.
55.
TOTALS
AVERAGE
120.0
50.092
.60
.60
055.
50.
01,
3.9 399.
09.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST D6-3
STACK OUTLET «1 BATTERY
TEST DATE
TB
TF
TT
NP
Y
DM
CP
PM
1
00 VM
OJ
TM
VMSTO
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
ENGLISH UNITS
12/13/81
945
1 145
120.0
12
.982
.404 IN
.84
.60 IN-H20
50.092 CU-FT
45.5 F
51.232 SCF
METRIC UNITS
12/13/81
945
1145
120.0
12
.982
10.3
.84
15.2
1.418
7.5
1.451
»»
PM-H20
CU-M
C
SO
AT STANDARD CONDITIONS*
VLC TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL,ML.
VMC VOLUME OF HATER VAPUR
AT STANDARD CONDITIONS*
BHO PERCENT MOISTURE BY VOLUME
FMD MOLE FRACTION DRY GAS
PC02 PERCENT C02 BY VOL., DRY
P02 PERCENT 02 BY VOL., DRY
PCO PERCENT CO BY VOL., DRV
PN2 PERCENT N2 BY VOL., DRY
MD MOLECULAR HT-OKY STACK GAS
MHS MOLECULAR XT-STACK GAS
147.1
6.924 SCF
147.1
.196 SCC
11.91
.681
5.10
11.00
.00
83.90
29.26
?7.92
11.91
.881
5.10
11.00
.00
83.90
29.26
27.92
-------
PB
PS1
PS
TS
VS
AS
OSSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLOW RATE, DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
29.79 IN-HG
-1.20 IN-H20
?9.70 IN-HG
455. F
16.4 FPS
7505. SO-IN
1546066. SCFH
3067686. ACFH
96.9
.0000
.00000 GR/OSCF*
.00000 LB/HR
756.67 HK-HG
-30.ae KM-H20
754.42 t>M-HG
235. C
5.0 *PS
4.842 SO-M
43837. SCKH
BbB68. ACHH
96.9
.0000
.0000 MG/DSCM
.000 KG/HR
EMISSION RATE
* 68 OEG F, 29.92 IN.HG.
•^
00
-------
EXAMPLE PARTICULATE CALCULATIONS TtST NU. D6-3
STACK OUTLET «\ BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD = (17.647 * VM • Y * (PB » PM / 13.6)) / (TM » 460.)
17.647 • 50.092 • .982 * ( 29.79 * .597 / 13.6)
VMSTD = - — — — — ...... - 51.232 OSCF
(
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SQRMVH * ITS » 460.))
VS a 85.49 * CP * OELP / tSQRT(M*S • PS) * PNTS)
VS * 85.19 * .84 * 78.678 / (SORT( 87.92 • 29.70) • 12. = 16.35 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
03 s VS * AS • 3600/144
OS s 16.35 • 7505. 3600/144 = 3067686. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
QSSTD = 17.647 * OS * PS * (1. • (8WO/100)) / (TS * 060.)
17.647 * 3067686. * 29.70 • (1. - (11.91/100))
OSSTD s ——— — ———-. ... ..... ..... —....— r 1548066. SCFH
( 455. » 460.)
> PERCENT ISOKINETIC
OT ISO * (305.58*(TS*460.))*((0.002669*VLC)+(VM*V*(PB»(P*/13.6))/(TM*460.)))/(TT*VS*PS*DN*DN)
(305.58*( 455.+460.))*((0.002669* 147.)*( 50.092* .982*1 29.79*( .597/13.6))/( 46.«460.)))
130 c ............— ..—......................—.....—. ....................................... x 96.88 PERCENT
120. • 16.35 * 29.70 * .404 • .404
PARTICIPATE LOADING — EPA METHOD s (AT STANDARD CONDITIONS)
CS * 0.001 * MN « 15.43 / VMSTO
CS * 0.001 * .0000 * 15.43 / 51.232 = .00000 GU/DSCF
PARTICULATE LBS/HR — EPA METHOD 5
PMR s CS * OSSTD / (15.43 * 453.6)
PMR « .00000 * 1548066. / (15.43 * 453.6) = .00000
-------
Run No. D6.3
Sample volume = 1.45 m . 51 .?3 scf
Example calculations
CS (Part) = 15.6/1.45 = 10.8 mg/m3
CS (Part) = 0.001 x 15.6 x 15.43/51.23 = O.QQ5 qr/dscf
CS (S02) =113.3/ 1.45= 7ft. 1 ma/m3
= 78.1 x 24.06/M_=_22_Ppm
= 0.001 xl!3.3 x 15.43/51.23 = 0.034 gr/dscf
. Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
15.6
1.0
1.4
0.0
113.3
7.5
2 Concentration,
mg/m
10.8
0.7
1.0
0.0
78.1
5.2
gr/dscf
0.005
0.0003
0.0004
0.000
0.034
0.002
ppm
29
1
A-487
-------
FIELD DATA
CD
CO
PLANT REPUBLIC STEEL
SAMPLING LOCATION STACK OUTLET U\
SAMPLE TYPE PARTICULAR
OPERATOR DAN FITZGEHALD
AMBIENT TEMP. (DEC. F) 13.
BAR. PRESS. (IN. HG) 29.79
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S) 3530411
STACK INSIDE DIM. (IN) 47.75 .00
PITOT TUBE COEFF. .84
THERM. NO. 133
LEAKAGE .002 CFM a) 3.
METER CALIB. FACTOR 1.033
READ ft RECORD DATA EVERY 10.0 MINUTES
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
eo.o
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
r* i nr* tt )
\f L.UL> n /
947
957
1007
1017
1027
1037
1047
1057
1107
1117
1127
1137
1147
GAS METER
READING
(CU.FT.)
VELOCITY
HEAD
(IN.H20)
CLEVELAND OHIO
BATTEHY
0 IN.HG
ORIFICE PRESSURE
DIFFERENT
(IN.H20)
IAL
STACK
TEMP
(DEG.F)
DESIRED ACTUAL
467.502
471.750
475.770
479.860
483.890
487.955
492.270
496.395
500.485
504.635
508.755
513.195
517.299
.050
.046
.048
,0«5
.046
.050
.047
.045
.047
.045
.050
.045
.64
.58
.60
.58
.58
.63
.60
.57
.59
.58
.64
.57
.64
.58
.60
.58
.58
.63
.60
.57
.59
.5*
.64
.57
455.
463.
465.
443.
455.
463.
447.
460.
460.
440.
448.
389.
DATE 12/13/81
RUN NUMBER D6-4
PROBE LENGTH ft TYPE 5 FOOT GLASS
NOZZLE : 1.0. .404
ASSUMED MOISTURE 13.7
SAMPLE BOX NUMBER
METER BOX NUMBER FB4
METER HEAD OIFF. 1.88
PROBE HEATER SETTING 400.
HEATER BOX SETTING 400.
K FACTOR 11628.3
DHY GAS METER
TEMP
(OEG.F)
INLET OUTLET
38. 38.
43. 40.
49. 42.
55. 45.
59. 48.
62. 52.
64. 54.
65. 55.
66. 57.
67. 58.
68. 60.
68. 60.
PUMP
VACUUM
(IN.HG)
2.0
1.5
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.5
2.0
SAMPLE
BOX TEMP
(DEG.F)
403.
444.
443.
440.
426.
433.
429.
438.
431.
425.
422.
387.
IMPINGER
TEMP
(DEG.F)
42.
48.
42.
45.
41.
46.
48.
52.
52.
55.
57.
55.
TOTALS
AVERAGE
120.0
49.797
.60
.60
449.
59.
51,
2.0
427.
49.
-------
PARTICIPATE FIELD DATA ft RESULTS TABULATION
PLANT* NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND OHIO DAN FITZGERALD
TEST D6-0
STACK OUTLET »\ BATTfcRY
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
>
*» VM
00
VO
TM
VMSTD
VLC
VMC
BHO
FMD
PC02
P02
PCO
pNe
MD
MWS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR XT-STACK GAS
ENGLISH UNITS
12/13/81
907
1107
120.0
12
1.033
.000 IN
.64
.60 IN-H20
09. 797 CU-FT
50.7 F
52. M7 SCF
161.7
7.611 SCF
12.60
.670
5.10
11.00
.00
83.90
29.26
27.83
METRIC UNITS
12/13/81
907
1107
120.0
12
1.033
10.3 CM
.80
15.2 *M-H20
1.010 CU-M
12.6 C
1.090 SCW
161.7
.216 SCM
12.60
.870
5.10
11.00
.00
83.90
29.26
27.83
-------
PB
PSI
PS
TS
VS
AS
QSSTO
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK bAS
STACK PRES. ABS.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE> DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINET1C
MG. EPA 5
EMISSION RATE
* 68 DEC F, 29.92 IN.HG.
29.79 1N-HG
-1.20 IN-H20
39.70 IN-HG
449. F
16.3 FPS
7505. SQ-IN
15A2579. SCFH
3062194. ACFH
99.9
.0000
.00000 GR/DSCF*
.00000 LB/HR
7b6.67 fH-HG
-30.«8 VV-H20
75a.42 KM»HG
232. C
5.0 PPS
4.642 SO-M
43b81. SCMH
8h712. *CVH
99.9
.0000
.0000 MG/OSCM
.000 KG/HR
*>
y?
o
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. D6-4
STACK OUTLET 01 BATTERY
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO s (17.647 * VM * Y « (PB * PM / 13.6)) / (TM » 460.)
17.647 * 49.797 * 1.033 * ( 29.79 * .597 / 13.6)
VMSTO s ...... . s 52.617 DSCF
( 55. » 460.)
VOLUME OF HATER VAPOR AT STANDARD CONDITIONS
VMC s .04707 * VLC
VMC 3 .04707 * 162. z 7.61 SCF
PERCENT MOISTURE IN STACK GAS
BNO s (100. * VMC) / (VMSTO * VNC)
100. * 7.61
BMO z ~—...................... - 12.64 PERCENT
52.617 + 7.61
MOLE FRACTION OF DRV STACK GAS
FMO 3 (100. > BMO) / 100.
100. . 12.6
FMD 3 ....................... 3 .874
100.
AVERAGE MOLECULAR MEIGHT OF DRY STACK GAS
MD 3 (PC02 * .44) * (P02 * .32) «• (PN2 * PCO) • .28
MD 3 ( 5.10*44/100) + (11.0*32/100) » ((83.9+ .0) * 28/100 z 29.26
MOLECULAR HEIGHT OF STACK GAS
MHS 3 MD * (1. - (BHO/100)) + 18. • (BfO/lUO)
MMS 3 29.26* (1. -(12.64/100)) «• 18. * (12.64/100) 3 27.83
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP = SUM. OF THE St)RT(VH * (TS + 060.))
VS s 85.09 • CP • OELP / (SORT(M*S * PS) * PNTS)
VS a 85.09 • .80 • 78.021 / (StJRH 37.83 * 89.70) * 12. = 16.32 FPS
STACK GAS VOLUMETRIC FLOH AT STACK CONDITIONS
OS * VS * AS • 3600/140
OS * 16.32 • 7505. 3600/100 c 3062190. ACFH
STACK GAS VOLUMETRIC FLOW AT STANDARD CONDITIONS
OSSTO * IT.607 * OS • PS * (1. - (BWO/100)) / (TS * 060.)
17.607 * 3062190. * 29.70 * (1. - (12.60/100))
OSSTD = 2 1502579. SCFH
( 009. » 060.)
p PERCENT ISOKINETIC
*» ISO s (305.58*(TS*060.))*((0.002669*VLC)+(VM*Y*(PB*(PM/13.6))/(TM+060.)))/(TT*VS«PS*DN*DN)
VO
^ (305.58*( 009.+060.))*((0.002669* 162.)+( 09.797*1.033*( 29.79»( .597/13.6))/( 55.+060.)))
ISO * .............. . ...... —............... ...................... .............. s 99.85 PERCENT
120. * 16.32 * 29.70 * .000 * .000
PARTICIPATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS * 0.001 • MN * 15.03 / VMSTD
CS z 0.001 * .0000 * 15.03 / 52.617 = .00000 GR/DSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR s CS • OSSTD / (15.03 * 053.6)
PMH s .00000 * 1502579. / (15.03 * 053.6) = .00000
-------
Run No. D6-4
Sample volume =1.49 m352.62 scf
Example calculations
CS (Part) =12.0/1.49= 8.0 mq/m3
CS (Part) = 0.001 x^-0 x 15.43/52.62= 0.004 qr/dscf
CS (S02) = / = mg/m3
= x 24.06/ = ppm
= 0.001 x
.x 15.43/.
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04-2H20
Water soluble sul fates
As S0a=
Sulfur dioxide
Sul f uric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
12.0
0.0
0.0
0.0
144.2
2.8
77
2 Concentration,
mg/m
8.0
0.0
0.0
0.0
96.8
1.9
51.7
gr/dscf
0.004
0.000
0.000
0.000
0.042
0.0008
0.022a
ppm
I PA contaminated.
A-493
-------
FIELD DATA
PLANT REPUBLIC STEEL
SAMPLING LOCATION COKE STACK
SAMPLE TYPE M5-250
OPERATOR 00
AMBIENT TEMP.(OEG.F) 32.
BAR. PRESS. (IN. HG) 29.79
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S)
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE CUEFF. .83
THERM. NO.
LEAKAGE .000 CFM a) 3.
METER CALIB. FACTOR .992
READ K RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
ft nt* w \
LLULK 1
945
955
1005
1015
1025
1035
1045
1055
1105
1115
1125
1135
1145
EVERY 10.0
GAS METER
READING
(CU.FT.)
191.991
197.190
202.330
207.560
212.780
218.010
223.260
228. 510
233.810
239.120
24a.430
249.750
255.077
MINUTES
VELOCITY
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
H20)
ACTUAL
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
.89
STACK
TEMP
(DEG.F)
455.
463.
465.
443.
455.
463.
447.
460.
460.
440.
448.
461.
DATE 12/13/81
HUN NUMBER D6-5
PBUBfc LENGTH S TYPE 6* GLASS
NUZZLE : I.U. .431
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBER FBI
METER HEAD DIFF. 1.37
C FACTOR .86
PROBE HEATER SETTING 250.
HEATER BOX SETTING 250.
REFERENCE PRESS. DIFF. .10
DRY GAS METER
TEMP
(DEG.F)
ULET OUTLET
37. 33.
41. 33.
49. 35.
55. 37.
59. 40.
62. 43.
63. 45.
65. 46.
65. 48.
66. 48.
67. 49.
67. 50.
PUMP
VACUUM
(IN.HG)
2.1
2.1
2.2
2.2
2.2
2.2
2.2
2.3
2.2
2.2
2.2
2.2
SAMPLE
BOX TEMP
(DEG.F)
271.
251.
289.
275.
267.
273.
258.
267.
266.
265.
264.
263.
IMPINGER
TEMP
(OEG.F)
42.
42.
43.
44.
44.
44.
46.
47.
48.
48.
48.
50.
TOTALS
AVERAGE
120.0
63.086
.89
.89 455,
58.
42.
2.2
267.
46.
-------
PARTICIPATE FIELD DATA A RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND no
TEST 06-5
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
> VM
>t»
VD
01 TM
VMSTD
VLC
VHC
BMO
FMO
PC02
poa
PCO
PN2
HO
MW3
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF HATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR HT-ORY STACK GAS
MOLECULAR WT-STACK GAS
ENGLISH UNITS
12/13/Bi
905
lias
120.0
IS
.992
.031 IN
.83
.89 IN-H20
63.086 CU-FT
50.1 F
64.634 SCF
191.1
8.995 SCF
12.22
.878
5.10
11.00
.00
83.90
29.26
27.88
METRIC UNITS
12/13/81
945
1145
120.0
12
.992
10.9
.83
22.6
1 .786
10.1
1.830
191.1
.255
12.22
.878
5.10
11.00
.00
83.90
29.26
27.88
*M
KM-H20
CU-M
C
sec
sen
-------
PB
P3I
PS
TS
VS
AS
OSSTO
OS
ISO
HN
CS
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRES, ABS.
AVERAGE STACK TEMP
AV6 STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE, ORT*
ACTUAL STACK FLOW RATE
PERCENT ISOKINEUC
MG. EPA 5
29.79 IN-HG
-1.20 IN-H20
29.70 IN-HG
«55. F
16.7 FPS
7066. SO-IN
1565391. SCFH
3112999. ACFH
105.7
.0000
.00000 GR/DSCF*
.00000 LB/HR
756.67 VM-HG
-30.18 VM-H20
754.«2 *M-MG
235. C
5.1 *PS
a.817 SO-M
VD
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 06-5
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTD * (17.647 • VM * Y * (PB + PM / 13.6)) / (TM » 460.)
17.647 * 63.066 • .992 • ( 29.79 » .890 / 13.6)
VMSTD = ———-.———.................. ... ... —. 64.634 DSCF
I 50. * 460.)
VOLUME OF MATER VAPOR AT STANDARD CONDITIONS
VNC s .04707 • VLC
VNC « .04707 * 191. z 9.00 SCF
PERCENT MOISTURE IN STACK GAS
~ BHO 8 (100. * VNC) / (VMSTD » VNC)
100. * 9.00
> BMO s s 12.22 PERCENT
J., 64.634 » 9.00
VD
~J
MOLE FRACTION OF DRY STACK GAS
FMD • (100. - BMO) / 100.
100. • 12.2
FMD » •••—................. z .678
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD e (PC02 • .44) * (P02 • .32) •» (PN2 » PCO) * .28
MD z ( 5.10*44/100) * (11.0*32/100) + KB3.9+ .0) • 28/100 = 29.26
MOLECULAR WEIGHT OF STACK GAS
MMS z MD * (1. • (BMO/100)) * 18. * (BftO/100)
MMS = 29.26* (1. -(12.22/100)) * 18. * (12.22/100) = 27.88
-------
STACK GAS VELOCITY AT STACK CONDITIONS
DELP * SUM. OF THE SORT(VH * (TS * 460.))
VS » 85.49 * CP * OELP / (SQRT(MHS * PS) * PNTS)
VS = 65.49 * .63 * 61.166 / (SORT( 27.88 • 29.70) * 12. = 16.68 FPS
STACK GAS VOLUMETRIC FLO* AT STACK CONDITIONS
OS : VS * AS * 3600/144
OS a 16.66 * 7466. 3600/144 a 3112999. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTD * 17.647 * OS * PS * (I. - (BWU/100)) / (TS * 460.)
17.647 • 3112999. * 29.70 * (1. - (12.22/100))
OSSTD = ———————............ ...—..... —........ = 1565391. SCFH
( 455. +• 460.)
> PERCENT ISOKINETIC
I
^ ISO « (305.58*(TS»460.))*((0.002669*VLC)«(VM*Y*(PB«(PM/13.6))/(TM*460.)))/(TT*VS*PS*UN*DN)
CO
(305.58*( 455.+460.))*((0.002669* 191.)»{ 63.066* .992M 29.79*( .890/13.6))/( 50.«060.)))
ISO a . . . — = 105.66 PERCENT
120. * 16.68 * 29.70 * .431 * .431
PARTICULATE LOADING — EPA METHOD 5 (AT STANDARD CONDITIONS)
CS a 0.001 * MN • 15.43 / VMSTO
CS s 0.001 * .0000 * 15.43 / 64.634 = .00000 GR/DSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR s CS * OSSTO / (15.43 * 453.6)
" PMR = .00000 * 1565391. / (15.43 • 453.6) s .00000
-------
Run No. D6.5
Sample volume =1.83 m T 64.63 scf
Example calculations
CS (Part) =19.9/1.83 = 10.9 mq/m3
CS (Part) = 0.001 x!9.9 x 15.43/64.63 = 0.005 qr/dscf
CS (S02) = /.
. mg/nT
x 24.06/_
.ppm
= 0.001 x
.x 15.43/.
gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
19.9
13.6
12.8
11.5
11.3
4.4
0.0
0.0
0.0
10.0
2.4
8.0
3 Concentration,
mg/m
10.9
7.4
7.0
6.3
6.2
2.4
0.0
0.0
0.0
5.5
1.3
4.4
gr/dscf
0.005
0.003
0.003
0.003
0.003
0.001
0.000
0.000
0.000
0.002
0.0006
0.002
ppm
A-499
-------
FIELD DATA
O
O
PLANT REPUBLIC STEtL
SAMPLING LOCATION CUKE STACK
SAMPLE TYPE M8-600
OPERATOR DO
AMBIENT TEMP. (DEG.F) 32.
BAR. PRESS. (IN.HG) 29.79
STATIC PRESS. (IN. H20) -1.20
FILTER NUMBER(S)
STACK INSIDE DIM. (IN) 97.50 .00
PITOT TUBE COEFF. .83
THERM. NO.
LEAKAGE .000 CFM * 7.
METER CALIB. FACTOR .967
READ & RECORD DATA
TRAVERSE
POINT
NO.
INIT
SAMPLE
TIME
(MIN.)
0
10.0
20.0
30.0
40.0
50.0
60.0
70.0
80.0
90.0
100.0
110.0
120.0
CLOCK
TIME
(24-HR
946
956
1006
1016
1026
1036
1046
1056
1106
1116
1126
1136
1146
EVERY 10.0
GAS METER
READING
(CU.FT.)
938.892
943.070
947.250
951.440
955.650
959. BIO
964.000
968.220
972.420
976.620
980.820
985.060
989.293
MINUTES
VELOCITY
HEAD
(IN.H20)
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
.050
CLEVELAND
0 IN.HG
ORIFICE
PRESSURE
DIFFERENTIAL
(IN.
DESIRED
.43
.43
.43
.43
.43
.43
.43
.43
.43
.43
.43
.43
H20)
ACTUAL
.43
.43
.43
.03
.03
.43
.43
.43
.43
.43
.43
.43
STACK
TEMP
(DEG.F)
455.
463.
465.
443.
455.
063.
447.
460.
460.
440.
048.
461.
DATE 12/13/81
RUN NUMBER 06-6
PROBE LENGTH ft TYPE 4* GLASS
NOZZLE : I.D. .378
ASSUMED MOISTURE 11.0
SAMPLE BOX NUMBER
METER BOX NUMBER FB6
METER HEAD OIFF. 1.51
C FACTOR .70
PRUBE HEATER SETTING 600.
HEATER BOX SETTING 600.
REFERENCE PRESS. OIFF. .21
DRY GAS METER
TEMP
(DEG.F)
INLET OUTLET
33. 35.
35. 35.
40. 35.
44. 36.
47. 37.
48. 38.
49. 39.
50. 00.
50. 00.
51. 01.
51. 01.
51. 41.
PUMP
VACUUM
(IN.HG)
3.5
3.8
3.9
3.8
4.0
4.9
5.4
5.6
5.7
5.8
6.5
6.8
SAMPLE
BOX TEMP
(OEG.F)
568.
598.
622.
612.
610.
611.
613.
615.
613.
613.
606.
605.
IMPINGER
TEMP
(DEG.F)
40.
40.
41.
41.
42.
42.
43.
44.
46.
Oh.
08.
51.
TOTALS
AVERAGE
120.0
50.001
.43
.43 455.
46.
38.
5.0 607.
44.
-------
PARTICULATE FIELD DATA ft RESULTS TABULATION
PLANT- NAME AND ADDRESS TEST TEAM LEADER
REPUBLIC STEEL CLEVELAND DO
TEST D6-6
COKE STACK
TEST DATE
TB
TF
TT
NP
Y
ON
CP
PM
1
Ln
0 VM
TM
VMSTO
Vlt
VNC
BNO
FMD
PC02
P02
PCO
PN2
MD
MMS
TIME-START
TIME-FINISH
NET TIME OF TEST, MIN.
NET SAMPLING POINTS
METER CALIBRATION FACTOR
SAMPLING NOZZLE DIAMETER
PITOT TUBE COEFFICIENT
AVERAGE ORIFICE PRESSURE
DROP
VOLUME OF DRY GAS SAMPLED
AT METER CONDITIONS
AVERAGE GAS METER TEMP
VOLUME OF DRY GAS SAMPLED
AT STANDARD CONDITIONS*
TOTAL H20 COLLECTED IN
IMPINGERS AND SILICA GEL, ML.
VOLUME OF NATER VAPOR
AT STANDARD CONDITIONS*
PERCENT MOISTURE BY VOLUME
MOLE FRACTION DRV GAS
PERCENT C02 BY VOL., DRY
PERCENT 02 BY VOL., DRY
PERCENT CO BY VOL., DRY
PERCENT N2 BY VOL., DRY
MOLECULAR NT-DRY STACK GAS
MOLECULAR NT-STACK GAS
ENGLISH UNITS
12/13/81
946
1146
120.0
12
.967
.378 IN
.83
.43 IN-H20
50.401 CU-FT
42.0 F
51.098 SCF
149.2
7.023 SCF
12.08
.879
5.10
11.00
.00
83.90
29.26
27.90
METRIC UNITS
12/13/81
94b
1146
120.0
12
.967
9.6
.83
10.9
1.427
5.5
1.447
149.2
.199
12.08
.879
5.10
11.00
.00
83.90
29.26
27.90
KM
MM-H20
CU-M
C
SCf
SCP
-------
PB
PSI
PS
TS
V3
AS
QSSTD
OS
ISO
MN
cs
PMR
BAROMETRIC PRESSURE
STATIC PRES OF STACK GAS
STACK PRESr A8S.
AVERAGE STACK TEMP
AVG STACK GAS VELOCITY
STACK AREA
STACK FLO* RATE* DRY*
ACTUAL STACK FLOW RATE
PERCENT ISOKINETIC
MG. EPA 5
EMISSION RATE
* 68 DEG F, 29.93 IN.HG.
29.79 IN-HG
-1.20 IN-H20
29.70 IN-HG
455. F
16.7 FPS
7466. SO-IN
1567349. SCFH
3112161. ACFH
108.5
.0000 r
.00000 GR/DSCF*
.00000 LB/HR
756.67 KM-HG
-30.48 KM-H20
754.42 PM-HG
235. C
5.1 fPS
4.817 SQ-M
44383. SCVH
88127. ACMH
108.5
.0000
.0000 MG/DSCM
.000 KG/HR
-------
EXAMPLE PARTICULATE CALCULATIONS TEST NO. 06-6
COKE STACK
VOLUME OF DRY GAS SAMPLED AT STANDARD CONDITIONS
VMSTO * (17.647 • VM • Y * (PB * PM / 13.6)) / (TM * 460.)
17.647 • 50.401 • .967 * ( 29.79 » .430 / 13.6)
VMSTD « ————— — — .-——..............—... = 51.098 DSCF
( 42. * 460.)
VOLUME OF WATER VAPOR AT STANDARD CONDITIONS
VXC = .04707 * VLC
VMC » .04707 * 149. = 7.02 SCF
PERCENT MOISTURE IN STACK GAS
8x0 » (100. • VWC) / (VMSTD * VNC)
100. * 7.02
> BNO e -—————- — — - — -. = 12.08 PERCENT
I 51.098 «• 7.02
Ui
. o
co
MOLE FRACTION OF DRY STACK GAS
FMD s (100. - BMO) / 100.
100. - 12.1
FMD » ———————— : .879
100.
AVERAGE MOLECULAR HEIGHT OF DRY STACK GAS
MD x (PC02 * .44) * (P02 • .32) * (PN2 •» PCO) • .28
MO * ( 5.10*44/100) •» (11.0*32/100) » ((83.9+ .0) * 28/100 = 29.26
MOLECULAR HEIGHT OF STACK GAS
MMS z MD * (1. - (BHO/100)) » 18. • (B*0/10U)
MHS = 29.26* (1. -(12.08/100)) » 18. * (12.08/100) * 27.90
-------
STACK GAS VELOCITY AT STACK CONDITIONS
OELP = SUM. OF THE SORT(VH * (TS * 360.))
VS a 85.09 • CP * OELP / (SU»T(MHS * PS) • PNTS)
VS s 85.49 * .83 * B1.166 / (SO»T( 27.90 • 29.70) » 12. - 16.67 FPS
STACK GAS VOLUMETRIC FLOW AT STACK CONDITIONS
OS = VS * AS * 3600/100
OS = 16.67 * 7466. 3600/144 = 3112161. ACFH
STACK GAS VOLUMETRIC FLON AT STANDARD CONDITIONS
OSSTO = 17.647 * OS * PS * (1. - (BHO/100)) / (TS + 460.)
17.647 * 3112161. • 29.70 * (1. - (12.08/100))
OSSTD = — = 1567349. SCFH
( 455. » 460.)
PERCENT ISOKINETIC
^ ISO = (305.58*(TS*460.))*((0.002669*VLC)*(VM*Y«(PB*(PM/13.6))/(TM«460.)))/(TT«VS*PS*DN«ON)
O
*• (305.5B*( 455.4460.))*((0.002669* 149.)+( 50.401* .967*( 29.79+( .430/13.6))/( 42.4460.)))
ISO = ———.................... ..............—..... ....................................... = 108.46 PERCENT
120. * 16.67 * 29.70 * .378 • .378
PARTICIPATE LOADING -- EPA METHOD 5 (AT STANDARD CONDITIONS)
CS = 0.001 * MN • 15.43 / VMSTD
CS > 0.001 * .0000 * 15.43 / 51.098 = .00000 GR/DSCF
PARTICULATE LBS/HR -- EPA METHOD 5
PMR = CS • OSSTD / (15.43 * 453.6)
PMR s .00000 * 1567349. / (15.43 * 453.6) « .00000
-------
Run No. D6.6
Sample volume = 1.45 m3.51.10 scf
Example calculations
CS (Part) = 9.2 /1.45= 6.3 mq/m3
CS (Part) = 0.001 x 9.2 x 15.43/51.10= 0.003 qr/dscf
CS (S02) =110.1/1.45= 75.9 mq/m3
= 75.9 x 24.0(5/64 = 28 ppm
= 0.001 x IIO.Ix 15.43/51.0 = 0.033 gr/dscf
Parameter
Particulate following
conditioning at:
Ambient
2-h at 350°F
4-h at 350°F
2-h at 400°F
4-h at 400°F
2-h at 600°F
Acid sul fates
As H2S04
As H2S04.2H20
Water soluble sul fates
As S04=
Sulfur dioxide
Sulfuric acid mist
As H2S04
Inorganic condensibles
Organic condensibles
TOC (Condensible)
Catch weight,
mg
9.2
0.2
0.3
0.0
110.1
11.4
o Concentration,
mg/m
6.3
0.1
0.2
0.0
75.9
7.9
gr/dscf
0.003
0.0001
0.0001
0.000
0.033
0.003
ppm
28
2
, A-505
------- |