United States
Environmental Protection
Agency
Air
Office of Air Quality
Planning and Standards
Research Triangle Park'NC 27711
EMB Report 78-NHF-2
February 1970
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SOURCE EMISSIONS TEST REPORT
OCCIDENTAL CHEMICAL COMPANY
Houston, Texas
AMMONIUM SULFATE DRYER BAGHOUSE EXHAUST STACK
Barry L. Jackson
Supervi sor
Ai r Test i ng
RFW W.O. #0300-81-04
Contract No. 68-02-2816
Work Assignment No. 2
JU
Peter J. Marks
Department Manager
Laboratory Services
for: ROY F. WESTON
Prepared by:
ROY F. WESTON
ENVIRONMENTAL CONSULTANTS-DESIGNERS
Weston Way
West Chester, Pennsylvania 19380
692-3030
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TABLE OF CONTENTS
PAGE
LIST OF TABLES AND FIGURES i
SUMMARY 1
INTRODUCTION 3
DESCRIPTION OF PROCESS 5
DESCRIPTION OF TEST LOCATIONS 7
Ammonium Sulfate Dryer Baghouse Inlet Duct . 7
Ammonium Sulfate Dryer Baghouse Exhaust Stack 7
DESCRIPTION OF SAMPLING TRAINS 10
Particulate Sampling Trains 10
Particle Sizing Train 11
TEST PROCEDURES 14
Preliminary Tests 1iป
Ammonium Sulfate Dryer Baghouse Inlet Duct 1^
Ammonium Sulfate Dryer Baghouse Exhaust Stack 15
ANALYTICAL PROCEDURES ' .16
Particulate Sample Recovery 16
Particulate Analyses 16
Particle Size Sample Recovery and Analyses 17
DISCUSSION OF TEST RESULTS 18
APPENDIX A - Raw Test Data
APPENDIX B - Laboratory Reports
APPENDIX C - Sample Calculations
APPENDIX D - Equipment Calibration Data
APPENDIX E - Detailed Baghouse Information
APPENDIX F - Project Participants
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TABLE
NO.
1
TITLE
Ammoniurn .Sulfate Dryer Inlet Duct
Summary of Test Data
Ammonium Sulfate Dryer Exhuast Stack
Summary of Test Data
Ammonium Sulfate Dryer Inlet Duct
Summary of Test Results
Ammonium Sulfate Dryer Exhuast Stack
Summary of Test Results
LIST OF TABLES AND FIGURES
PAGE
20
21
22
23
FIGURE
NO.
1
2
TITLE
Ajrimon i urn Sul fate Dryer and Baghouse
Ammonium Sulfate Dryer Baghouse Inlet Duct
Port and Sampling Point Locations
Ammonium Sulfate Dryer Baghouse Exhaust Stack
Port and Sampling Point Locations
Particulate Sampling Train
EPA Method 5
Baghouse Inlet Duct
Particulate Sampling Train
EPA Method 5
Baghcuse Exhaust Stack
Ammonium Sulfate Dryer Baghouse Inlet Duct
Particle Size Distribution
PAGE
6
8
12
13
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SUMMARY
The Emission Measurement Branch of the U. S. Environmental Protection
Agency contracted Roy F. Weston, Inc. to conduct a source testing and
analysis program at Occidental Chemical Company's Houston, Texas
Ammonium Sulfate Plant.
The primary objective of the testing program was to quantify the
participate emissions to the atmosphere from the Ammonium Sulfate
Dryer Baghouse Stack. This objective was achieved by performing a
series of three particulate tests utilizing EPA Method 5 procedures
at the baghouse exhaust stack location. In addition, visual determinations
of plume opacities were made simultaneously with each particulate test at
(2)
the source discharge point according to EPA Method 9 protocol. Also,
EPA Method 5 particulate tests were executed at the baghouse inlet
site simultaneously with the exhaust stack tests to measure the potential
uncontrolled emissions and to calculate particulate removal efficiencies.
n
A singular Anderson cascade impactor test was conducted at the baghouse
inlet location to determine the particle size distribution of the
entering particulate matter.
The particulate matter emission results are summarized below:
Ammonium Sulfate Dryer Baghouse
Particulate Concentration
Grains/DSCF Pounds/Hour
Test
No.
1
2
3
Date
9/12/78
9/12/78
9/12/78
9/12/78
9/13/78
9/13/78
Test
Locat ion
Inlet Duct
Exhaust Stack
Inlet Duct
Exhaust Stack
Inlet Duct
Exhaust Stack
1.01
0.028
0.96
0.085
3-83
0.093
8.36
0.24
7.84
0.70
31.2
0.74
Part iculat
Removal
Eff i ci ency
Percent
97.2
91.1
97-6
^ 'Code of Federal Regulations, Title kQ, Part 60, Appendix A, "Standards of
Performance for New Stationary Sources," August 18, 1977-
(^Federal Register, Vol. 39, No. 219, November 12, 1974.
(3)0p. Cit.
-------
No visible emissions were observed emanating from the baghouse exhaust
stack during the test program by the certified observer.
Figure 6 illustrates the particle size distribution of the particulate
matter at the baghouse inlet location.
Detailed summaries of test data and test results are presented in
Tables 1 through 4 of this report.
- 2 -
-------
INTRODUCTION
The Emission Measurement Branch of the U. S. Environmental Protection
Agency contracted Roy F. Western, Inc. to conduct a source testing and
analysis program at Occidental Chemical Company's Houston, Texas
Ammonium Sulfate Plant.- The objective of the testing program was to
measure various emission parameters from Oxychem's Ammonium Sulfate
Dryer.
The location tested, plus the number and types of tests performed at
each site are listed below:
1. Ammonium Sulfate Dryer Baghouse Inlet Quct.
a. Three particulate tests by EPA Method 5-
b. One particle size distribution tes-t by cascade
D
impaction (Anderson ).
2. Ammonium .Sulfate Dryer Baghouse Exhaust Stack.
a. Three particulate tests by EPA Method 5> Each
particulate test .was performed simultaneously
with one of the inlet duct tests.
b. .Three opacity tests by EPA Method 9- Visual
determinations of plume opacities determined
concurrently with the particulate tests.
All tests were conducted during the period 12-13 September 1978 by Weston
personnel and were observed by Mr. Dennis P. Holzschun, EPA Technical
Manager.
Test data and test results are presented in Tables 1 through k of this
report. Particle size distribution results are shown in Figure 6. Also
incorporated herein is a description of the test locations, test equipment,
test procedures, sample" recovery, and analytical methods used during the
- 3 -
-------
test program. Raw test data, laboratory reports, sample calculations,
equipment calibration data, baghouse details, and a list of project
participants are provided in Appendices A through F, respectively.
-------
III. PROCESS DESCRIPTION AMD OPERATION
The: Occidental Chemi-ca'l plant produces ammonium sulfate (AS) from ammonia
and sulfun'c acid. ATI of the AS produced is sold for use as a fertilizer. The
plant, did not operato continuously during 1978 due to problems with sulfuric
acid supply and cyclical market conditions for AS.
A. Process Description
Su "If uric acid and ammonia are combined in a crystal Vizer or saturator.
The reaction in the saturator to form the AS occurs with much evolution of
.heat. The reaction takes place in a medium.of "mother liquor"'which is a dilute
solution of AS. As the reaction proceeds and the concentration of AS in the
ir.other liquor increases, the solution becomes supersaturated, and the AS / '";.
begins to precipitate in the form of crystals. The crystals grow to about
1/8" diameter maximum and leave the saturator through bottom feed lines to
centrifuges, A slight, vacuum (ll.O psia) is maintained on the saturator
to aid evaporation.
At the centrifuges, the crystals are separated from the mother liquor
and are discharged as wet crystals onto a conveyor belt "leading to the
dryer. The mother liquor goes back to storage. The wet crystals contain
about 2 to 3 percent moisture at this point.
The dryer installed at this plant is a natural gas, direct-fired rotary
drum unit. The water content of the AS is reduced to a range of about
0.3 percent, to 0.5 percent. Some drying of AS also occurs on the lengthy
conveyor belt feeding the dryer. From the dryer the AS passes to a screening
operation where "granular" and "coarse" products are separated.
-------
The baghouse is a Carter Day unit Model Mo. 24RV60 containing ?>?.() square
feet of dacron felt cloth. It employs a periodic reverse jet of filtered
air to clean the bags. The AS collected drops into a conical bottom in
the housing and is pumped back, to the mother liquor tank after res'lurrying.
The bags in the baghousc had been replaced.during the week of September 4,
prior to the test.
A schematic diagram of the dryer and baghouse is presented in Figure 1.
B. Process Operation
The purpose of the test program was to measure emission levels from
the Occiden.tal. Chemical baghouse controlling the dryer. Process conditions
were carefully observed and testing was performed only during periods when
the plant was operating normally. During the tests, pertinent operating
conditions were monitored and recorded on process data sheets. This data is
summarized in Tables I-IV of Appendix B.
The plant was operating over 90 percent of its design capacity during
each of the three emission tests which were conducted. No calibrated weigh
belts were used at this plant. The production rate was determined most
accurately by a digital sulfuric acid flow meter which registered the total
.acid withdrawn from storage for a 24-hour period. The plant reported to be
operating with 94 - 95 percent I-LSCL.
The temperature of the exit gases from the dryer were read off a strip
chart in the control room. Temperatures of this strip chart were slightly
lower than those measured by the test team at the baghouse inlet. The temperature
and the centrifuge motor drive amperage were monitored during the emission tests
to establish the steady state operation of the dryer throughput rate. Other
process parameters monitored are. included in Appendix B. Tables I-IV.
-------
The -Pollowing parameters were monitored during the tests to verify
that the dryer was operating normally,
1. Acid flow rate and totalizer amount,
2. Ammonia flow rate.
3. Dryer outlet gas temperature.
4. Centrifuge amperes.
5. Temperature of the vapor leaving the saturator,.
6. Liquid level in the saturator (inverse reading).
"7. Liquid level in'the mother liquor tank".
8. Neutral point titration (ml of O.'IM NaOH).
9. Percent, solids in -the magma.
The raw data sheets for these parameters are included in .-./....' .
Table* I - IV.
Process monitoring for test No. 1 began at 9:50 a.m. on September 12,
1978, and continued until 12:35 p.m. The centrifuges were shut down for
20 minutes for water flushing of the centrifuge inlet lines. The AS
production ceased during this period but the acid and ammonia feed to the
saturator continued. Since the production rate obviously affected emissions,
the test team was advised immediately when the production stopped. Emission
sampling was stopped for the 20 minute period and resumed after a short
period to allow buildup of AS in the dryer.
-------
Monitoring for test Mo. 2 began at 1 r/l.O p.m. on September 12, 1978ป
and concluded at 4:20 p.m. Test No. 3 process monitoring began at 9:H> a.m.
on September 13, "1978, and concluded at 1:00 p.m. As with the first tests,
the emission sampling was suspended during centrifuge servicing.
-------
OCCIDENTAL CHEMICAL COMPANY
Houston, Texas
FIGURE 1
AMMONIUM SULFATE DRYER AND BAGHOUSE
Gas Flow to Atmosphere
A
Exhaust Stackฃ
Test Site
Inlet Duct
Test Site
Ammon i urn
Sul.fate
Dryer
Shelter
r
4 7
Baghouse
Fan
Product
- 6 -
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TABLE I
SUMMARY OF AS PRODUCTION RATE DATA
Test; No. 1
Average indicated acid rate, gpm
Standard Deviation, gpm
Equivalent AS production rate, Tons/hr ,
based, on .indicated acid rate
Acid rate from, totalizer, gpm
Equivalent AS production rate, Tons'/hr,
based on acid totalizer rate
Ammonia Rate, Ib/hr (average readout,
t e iTip er a t u r e c o r r e c t e d )
Standard Deviation, Ibs/hr
Equivalent: AS production rate, Tons/hr ,
based on ammonia rate
Ibs
A.S product 'conveyer sample rate,- -
1
31.67
.38
19 .. 1
28.8
17,4
8400
141
16 . 3
4.32
2
31.8
Small
17.6
29.0
16 . 4
8402
Small
16.3
3.90
3
34 .
Small
19.4
34.1
.20.6
843S
Small
r'
16.4
3.81
Equivalent AS production rate,Tons/hr,.
bas&u on AS product conveyor rate 18.7 16.9 16,6
-------
TABLE II
ADDITIONAL PROCESS PARAMETERS MONITORED DURING TEST NO. 1
Elapsed Time, ruin..
Sciturator Vapor Temp, F
Dryer Exit Air Temp, F
Percent Solids in the magma
Neutral Point Titration,
ml 0.1N NaOH
Centrifuge Current, Ampsres
Unit: #2
0 30 60 90 120 1/sO
182 182 182 182 '181 182
135 - 135 - 135 135
70 70 74 72
8.0
6.0
8.2 . 12.0
20
18
18 18
Unit v:3
18
23
25 25
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TABLE III
ADDITIONAL PROCESS PARAMETERS MONITORED DURING TEST NO. 2
Elapsed Time, rain.
S.o.turator Vapor Temp, F
Dryer Exit Air Temp, ฐF
Percant Solids in magma
Keutral Point Titration,
ir.l 0..1N NaOH .
0 30 60 90 ' 120 150
182 183 183 183 183 183
136 - 136 - 138 136
71 71 70 72 .71 7.1
7.8 7.8 7.8 7.8 7.8 7.8
Centrifuge Current, Ampere?
Unit ฃ2
Unit i/3
20
23
20
23
18
22
18
22
18
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TABLE IV
ADDITIONAL PROCESS PARAMETERS MONITORED DURING TEST NO. 3
Elapsed Time:, mia.
Sa&urator Vapor Te.inp, F
Dry-ar Exit Air Teran, F
Percent Solids in magma
Neutral Point Titration.
nil OV1N NaOH
0 30 60 90 120 150
182 182 182 182 182 183
136 . - 135 - 136 138
71 71 70 70 71 71
7.8 10.0
4.8 6.8 7.8
Centrifuge Current, Arr.pferes
Unit #2
Unit ฃ3
20
22
21 . 23 6'-.. 0 18
25 25 25 25 0-
*Shut.down - Unit No. 1 operating but ammeter was defective
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-------
DESCRIPTION OF TEST LOCATIONS
Ammonium Sulfate Dryer Baghouse Inlet Duct
Two 3" I-D. test ports approximately 90 apart were installed on a
straight section of the 11" I.D. stack at a location which v/as 5-0
stack diameters downstream and 2.3 diameters upstream from the
nearest gas stream flow disturbances. EPA Method 1 ^ criteria for
this test location required a minimum of 20 traverse points but due
to a heavy build-up of particulate matter cover ing -^68% of the
inside area of the duct the particulate tests were run at a single
point of average velocity during each of the three test runs. See
Figure 2 for port and sampling point locations.
Ammoniurn Su1 fate Dryer Baghouse Exhaust Stack
Two 3" I.D. test ports were placed on one side of the 7-1/2" x 8-5/8"
rectangular exhaust stack serving the baghouse. The ports were located
15 diameters downstream and 10 diameters upstream from the nearest flow
disturbances. Since the eight and two diameter criterion were met, a
minimum of eight traverse points were required by EPA Method 1
regulations. Figure 3 illustrates duct geometry plus port and sampling
point locations.
- 7 -
of Federal Regulations, Title ^0, Part 60, Appendix A, "Standards
of Performance for New Stationary Sources," August 18, 1977-
-------
Baghouse
Port X
FIGURE 2
OCCIDENTAL CHEMICAL COMPANY
Houston, Texas
AMMONIUM SULFATE DRYER BAGHOUSE INLET DUCT
PORT AND SAMPLING POINT LOCATIONS
Roof
Ammonium Sulfats
Dryer
Port Y
Blockage
Duct Cross-Sectional View
- 8 -
-------
OCCIDENTAL CHEMICAL COMPANY
Houston, Texas
FIGURE 3
AMMONIUM SULFATE DRYER BAGHOUSE EXHAUST STACK
r
0
0
ซ
9
0
o
0
9
T~
7-1/2" I.D
'
L
J
3-1/8"
3" f-
Duct Cross-Sectional View
Traverse
Point
Number
1
2
3
iป
Distance From
Inside Near
Wai 1 , Inches
1
2-3/4
A-5/8
6-1/2
oo
FAN
7-5'
METAL STACK
-------
DESCRIPTION OF SAMPLING TRAINS
Parti culate Sampling Trains
The test train utilized for participate sampling at the bag house inlet duct
location v/as the standard EPA Method Five Train (see Figure *<) .
A stainless steel nozzle was attached to a heated (.-^250 F) 3' borosilicate glass
probe which was connected directly to a borosilicate filter holder containing a
4" Reeve Angel 900 AF glass fiber filter. The filter holder v/as maintained at
o R
approximately 250 F in a heated chamber, and was connected by Tygon vacuum
tubing to the first of four Greenburg-Smith impingers which were included in
the train to condense the moisture in the gas stream. Each of the first two
impingers contained 100 ml of distilled water, the third was dry and the final
impinger contained 200 grams of dry pre-weighed silica gel. The first, third,
and fourth impingers were modified Greenburg-Smith type; the second was a standard,
Greenburg-Smith impinger. All impingers were maintained in a crushed ice bath.
A RAC control console with vacuum pump, dry gas meter, a calibrated orifice, and
inclined manometers completed the sampling train.
Flue gas temperature was measured by means of a Type K thermocouple which was
connected to a direct readout pyrometer.. The thermocouple sensor was positioned
adjacent to the sampling nozzle.
Gas velocity was measured using a calibrated "S" type pi tot tube provided with
extensions and fastened alongside the sampling probe. Gas stream composition
(carbon dioxide, oxygen, and carbon monoxide content) v/as determined utilizing
Orsat apparatus to analyze stack gas samples. Gas stream composition proved
to be ambient air since no combustion products were found in any of the stack
gas effluent samples.
The test train used for'particulate sampling at the baghouse exhaust stack
location was identical to the train described above except for a rigid
borosilicate connection in place of flexible tubing between the filter
- 10 -
-------
between the filter holder and the first impinger. See Figure 5 for
train schematic.
Part i cle _5 ize Distribution Sampling Apparatus
R
A stainless steel nozzle was connected directly to an 8-stage Anderson
cascade impaction device which separated the particles according to
their effective aerodynamic particle diameters. A glass fiber filter
was used to capture any particles that passed through the impactor
substrates to permit the measurement of total particulate. The filter
holder was maintained at stack temperature and was connected by Tygon
vacuum tubing to the first of four Greenburg-Smith impingers which were
included in the train to condense the moisture in the gas stream. All
impingers were maintained in a crushed ice bath. A RAC control console
with vacuum pump, dry gas meter, a. calibrated orifice, and inclined
manometers completed the sampling trai'n.
-------
0.75 TO 1 in.
TEMPERATURE SENSOR
2:0.75 in. PITOTTUBE
TEMPERATURE SENSOR
THERMOMETER
TEMPERATURE CONTROLLED
HEATED AREA
PITOT MANOMETER
ORIFACE
REVERSE-TYPE
PITOTTUBE
\
VACUUM GAUGE
MAIN VALVE
\
AIRTIGHT PUMP
CHECK VALVE
VACUUM
LINE
THERMOMETERS
DRY GAS METER
FIGURE k PARTICULATE SAMPLING TRAIN
EPA METHOD 5
BAGHQUSE INLET DUCT
-------
, TEMPERATURE
SENSOR
0.75 TO 1 in.
0.75 in.
PITOT TUBE '
PROBE
.TEMPERATURE SENSOR
, THERMOMETER
CHECK VALVE
VACUUM LINE
VACUUM GUAGE
/THERMOMETER
/HEATED AREA
FILTER HOLDER
THERMOMETERS
PROBE-(pi{
REVERSE-TYPE
PITOT TUDE
ORIFICE
AND
MANOMETER
PI TOT MANOMETER
ICE BATH
DISTILLED WATER
FIGURE 5 PART1CULATE SAMPLING TRA1N-EPA METHOD 5
EPA METHOD 5
BAGHOUSE EXHAUST STACK
-------
TEST PROCEDURES '
Preliminary Tests
Preliminary test data was obtained at each sampling location. Stack geometry
measurements were recorded and sampling point distances calculated. A pre-
liminary velocity traverse was performed at each test location utilizing a
.calibrated "S" type pi tot tube and a Dwyer inclined manometer to determine
velocity profiles. Stack gas temperatures were observed with a direct
read-out pyrometer equipped with a chromel-a 1umel thermocouple. Gas
stream composition and moisture content values were estimated from
information supplied by Oxychem.
Preliminary test data was used for nozzle sizing and nomagraph set-up for
isokinetic sampling .procedures.
Calibration of the probe nozzles, pitot tubes, metering systems, probe heaters,
temperature gauges and barometer were performed as specified in Section 5 of
EPA Method 5 test procedures (see Appendix E for calibration data).
Ammonium Sulfate Dryer Baghouse Inlet Duct
A series of three tests were conducted at the inlet, to the Ammonium Sulfate
Dryer Baghouse simultaneous with pฃ)rticulate test runs at the exhaust stack.1
The sampling was performed at one point of average velocity for a total test
time of 120 minutes. This point was chosen before each test by running a
rough velocity traverse across the open area of the duct. Test data was
recorded every five minutes during all test periods.
Table 1 presents a summary of test data for each of the three runs. Test
result summarization appears on Table 3-
-------
One particle size distribution test was performed following the completion
of test run 3.
One sampling point located at a site of average velo'city was selected from
velocity traverse data for particle size distribution testing. The gas
stream was sampled isokinetically at that point for k minutes which permitted
collection of sufficient sample for analysis without overloading the filter
substrates. Sample volume, temperature, and pressure data was recorded
before and after the test. See Figure 6 for a distribution plot.
Ammonium Sulfate Dryer Baghouse Exhaust Stack
A series of three EPA Method 5 tests were performed at the Ammonium Sulfate
Dryer Baghouse exhaust stack simultaneous with the inlet test runs. Eight
points were traversed, 4 per port axis, for 15 minutes each yielding a test
period 120 minutes in length.
During particulate sampling, gas stream velocities were measured by inserting a
calibrated "S" type pitot tube into the stream adjacent to the sampling nozzle.
The velocity pressure differential was observed immediately after positioning
the nozzle at each point, and sampling rates were adjusted to maintain isokinetic
sampling. Stack gas temperatures were also monitored at each point with the
pyrometer and thermocouple. Additional temperature, measurements were made at
the final impinger and at the inlet and outlet of the dry gas meter.
Test data was recorded every five minutes during all test periods. Table 2
presents a summary of test data for each of the three runs. Test result
summarization appears on Table A.
Visible emissions observations were recorded concurrently with each particulate
test repetition by a certified observer according to EPA Method 9 procedures.
See Table k for result 'summary.
-------
ANALYTICAL PROCEDURES
Particulate Sample Recovery
At the conclusion of each test, the sampling trains were dismantled,
openings sealed, and the components transported to the field laboratory.
Sample integrity was assured by maintaining chain of custody records
which will be supplied upon request.
A consistent procedure was employed for sample recovery:
o The glass fiber filter(s) was removed from its holder with
tweezers and placed in its original container (petri dish),
along with any loose particulate and filter fragments (Sample 1).
o The probe and nozzle were separated and the internal particulate
rinsed with acetone or distilled water into a borosilicate container
while brushing a minimum of three times until no visi'ble particles
remained. Particulate adhering to the brush was rinsed with acetone
or water into the same container. The front half of the filter
holder was rinsed with acetone or water while brushing a minimum
of three times. The rinses v/ere combined (Sample 2) and the
container sealed with a Teflon lined closure.
o The total liquid in impingers one, two and three was measured,
the value recorded, and the liquid discarded.
o The silica gel was removed from the last impinger and immediately
weighed.
o Acetone and distilled water samples were retained for blank
analys i s.
Particulate Analyses
The filters (Sample 1) and any loose fragments were desiccated for 2k hours and
weighed to the nearest 0.1 milligram to a constant weight.
- 16 -
-------
The acetone and distilled water wash samples (Sample 2) were evaporated
(acetone at ambient temperature and pressure; water at 105 C and ambient
pressure) in tared beakers, and desiccated to constant weight. All sample
residue weights were adjusted by the acetone or water blank values.
The weight of the material collected on the glass fiber filter(s) plus the
weight of the residue of the nozzle/probe/front-half filter holder washes
represents the "total" EPA Method 5 catch. Complete laboratory results
are presented in Appendix B of this report.
Particle Size. Sample Recovery and Analyses
The cascade impactor substrates and any loose fragments were carefully
removed from their support plates with tweezers and placed in individual
containers (petri dishes) for shipment to Weston Laboratory.
Each cascade impactor filter was fired at 525 C and pre-weighed to the
nearest 0.1 milligram to constant weight at Weston1s Laboratory prior
to on-site application. Subsequent to emissions exposure, the cascade
impactor substrates, back-up filters and any loose fragments (Sample ^i)
were desiccated for 2k hours in the Laboratory, and weighed to the nearest
0.1 milligram to constant weight.
- 17 -
-------
DISCUSSION OF TEST RESULTS
Participate test data and test result summaries are presented in Tables 1
through A of this report. Figure 6 illustrates the particle size
distribution of the participate matter at the baghouse inlet location.
No unusual process operating conditions were encountered during any of
the test periods.
A heavy build up of particulate matter covered approximately 68% of the
inside area of the baghouse inlet duct at the test port location and
therefore precluded particulate/velocity traversing of the duct cross-
sectional area as specified in EPA testing methodology (see Figure 2).
Sampling at a single point of average velocity proved to be the most
feasible testing alternative (the blockage could not be easily removed)
and was the procedure followed for all three inlet tests. Therefore,.
since no part iculate/veloc-i ty traversing could be performed as required
to insure representative sampling, the inlet test results should only
be viewed as a rough guide when evaluating the performance efficiency
of the bag collector.
The amount of particulate matter discharged to the atmosphere from the
baghouse was <_ 0.093 grains/dscf and ฃ Q.Jk pounds/hour. The certified
observer recorded no visible emissions emanating from the stack during
the test program. However, water droplets containing dissolved particulate
matter were frequently observed dripping from the stack during the test
periods. This phenomenon was due to water vapor condensation on the inside
walls of the stack due to cooling the gas stream below the saturation
temperature.
The particulate removal "efficiency of the baghouse was mediocre averaging
roughly 95-3%.
- 18 -
-------
D
Results of the Anderson cascade impaction particle size distribution test
conducted at the baghouse inlet site showed a perponderance of relatively
large particles entering the collector (90% of the particles, by weight,
were _>_ 2.2 y in diameter). Visual inspection of a sample collected from
the baghouse indicated the presence of many large product granules.
It is suspected that the high grain loading measured at the outlet
location was due to a malfunction in the baghouse. Consequently, the
plant was contacted, the baghouse corrections were made, and three
additional tests were run at the baghouse outlet location at a later
date. The inlet duct was not tested during this period since most of
the internal area of the duct was filled with an irregular buildup of
product solids at the test site which prevented representative sampling.
Since the entire unit would have been required to shut down to enable
the inlet duct to be cleaned a decision was made to test the outlet
location only.
- 19 -
-------
OCCIDENTAL CHEMICAL COMPANY
Hous ton , Texas
TABLE 1
AMMONIUM SULFATc DRYER BAGHCUSE INLET DUCT
Sunrcary of Te^st^ Data_
Test Para
Tes t Number
Test Date
Test Period
S a n p 1 i _n c _D j t a
Samp ling Duration, mf nutts
Nozzle Dia"-.-ter, inches
Baronetric Pressure, Inches mercury
Average Orifice Pressure Differential, inches water"
Average Dry Gas Temperature at Meter, ฐF
Samp Ie Vo!une at Meter Conditions, cubic feet
Somp I e Vo I ume at Standard Conditions, cubic
Gas Strga.n Mo if. tu/e Content
Tola J Water Collected by Train, ml
Standard Volume of Water Collected, cubic feet
Moisture In Cos Stream, percent by volume
Mole Fraction of Dry Gas
Gas _S t r e; a m Compos it i o n
C02, percont by vof'jme
Oo, percent by vol urne
CO, percen t by vo! u.~e
N'2 , percent by vo I UiT.e
Molecular Weight of Wet Gas
Molecular Weight of Dry Gas
Gas Stream Veloci t_y_
Static Pressure, inches water
Absolute Pressure, Inches mercury
Average Temperature, F
Pttot Tube Calibration Coefficient
Total Number of Sa;np! ing Points
Velocity at Actual Conditions, feet/second
GasS t ream Vo t erne t r ic^_F 1 oy/
Stack Cross-Sect Ional Area, square feet
Volumet rIc FIow at ActuaI Cord 11 ions, cub ic fee t/m i nute
Vol umetf" ic Flow at Standard Conditions, cubic feet/minute
Percent Isokinot ic
wa t e r
feet
ie t/m i nutc
feet/inute
1
9/12/73
O9'i0-1230
120.0
0.125
2S-77
0.55
86.
50.33
^9-37
156.
7.3^
12.9
0.871
0.0
20.9
0.0
79.1
27-55
28.97
- 2. it
29.59
153-
0.831
1.0
103.
0.21
1 ,300.
960.
2
9/12/73
1350-1620
120.0
0. 125
23.77
0.55
89.
W.37
<<7.27
I'd .5
6.66
12.lt
0.876
0.0
20.9
0.0
79.1
27:62
28.97
- 2.8
29-56
176.
0.331
1.0
105-
0.21
1 ,320.
950.
3
9/13/78
0315-1225
106.0
0. 125
29.79
0.55
89.
!<2.
-------
OCCIDENTAL CHEMICAL COMPANY
Houston, Texas
TABLE 2
AMMONIUM SULFATE DRYER SAGHOUSE EXHAUST STACK
Sumnary of Test Data
Test Data
Test Number
Test Date
Test Period
Samp I in-; Data
Sampling Duration, minutes
Nozzle Diameter, inches
Barometric Pressure, inches mercury
Average Orifice Pressure Differential, inches water
Average Dry Gas Temperature at Meter, ฐF
Sample Volume at Meter Conditions, cubic feet
Sample Volume at Standard Conditions, cubic feet
Gas Stream Moisture Content
Total Water Collected by Train, ml
Standard Volume of Water Collected, cubic feet
Moisture in Gas Stream, percent by volume
Mole Fraction of Dry Gas
Gas Stream Composition
CG"2, percent by volume
0^, percent by volume
CO, percent by volume
(12, percent by volume
Molecular Weight of Wet Gas
Molecular Weight of Dry Gas
Gas Stream Veloci tv
Static Pressure, inches water
Absolute Pressure, inches mercury
Average Temperature, F
Pitot Tube Calibration Coefficient
Total Number of Sampling Points
Velocity at Actual Conditions, feet/second
Gas Stream Volumetric Flow
9/12/78
0940-1230
120.0
0.189
29-77
0.69
85.
56.60
186.
S.76
13.7
0.363
2
9/12/73
1350-1620
120.0
0.185
29.77
0.60
39.
52..-8
51.03
6.83
11.8
0.882
9/13/7S
0915-1225
120.0
0.189
29-79
0.55
87.
5L27
1<*7.5
6.9
-------
OCCIDENTAL CHEMICAL COMPANY
Houston, Texas
TABLE 3 '
AMMONIUM SULFATE SAGHOUSH INLET DUCT
Senna ry or Test P.esu } t s
Test Data
Test Murnber
Test Dace
Test Time
Gas Flow
Standard Cubic Feet/minute, dry
Actual Cubic Feet/minute, wet
Par t i cu I a t S5
Nozzle, Probe and Front Hair" Filter Holder Catch Fraction, g
Filter Catch Fraction, g
Total Pa.-t iculates, g
Particuiote Emissions
Grains/dry standard cubic foot
Pounds/hour
Baghouse Participate Removal Efficiency, percent
Product Moisture Content
Moisture content of Dryer Inlet Sampla, percent
Moisture content of Dryer Outlet Sample, percent
1
9/12/78
OSAO-1230
960.
1 ,300.
2.7212
0.520^
3. 2*116
1 .01
8.36
97.2
0.46
0.14
2
9/12/78
1350-1620
950.
1,320.
2.5637
0,3817
Z.W*
0.96
7.31.
91.1
0.50
0.19
3
9/13/73
0915-1225
950.
1 ,320.
7.2971
2.3?21
1.0.2S92
3-33
31.2
97.6
0.54
0.03
Based on Total P^rticulates captured by t ra i n.
Standard Conditions - 68ฐ? and 29-32 inches mercury.
-------
OCCIDENTAL CHEMICAL COMPANY
Hous con, Texas
TA3LE It
AMMONIUM S'JLFATE DRYER BAGHOUSE EXHAUST STACK
Sunimarv of Test Results
Test Data
Test Number
Test Date
Test Ti.ne
Gas Flow
Standard Cubic Feet/minute , dry
Part i cut act's
Mo:;lc:, Probe and Front Half Filter Holder Catch Fraction, g
Filter Catch Fraction, g
Total Part iculates , g
Particulate Emissions
Grains/dry standard cubic foot"
Pounds/hour
Saghouse Particular Removal Efficiency, percent
Visible Em i s s i on s
> S percent opacity, minutes observed
0 percent opacity, ninutes observed
No visible emission, minutes observed
Product Moisture Content
"loir.ture content of Dryer Inlet Sample, percent
Moisture content of Cryer Outlet Sample, percent
1
9/12/78
09^0-1230
930.
> o:! A
i , .iou .
0.059!)
0.0
-------
AMMONIUM SULFATE DRYER BAGHOUSE INLET
Particle Size Distribution
FIGURE 6
10 0
q n
y . u
8 0
7 n
/ . u
A n
in b'U
ฃ en
o
. i. n
r= H .U
F, ? n
uu
2:
- u /
o 0 A
CC
^ n q
uu ,
-=. n L.
K
CJ
uj n ^
u_ u >
u.
LU
00
. i.
0.1
/
/
/
/
/
/
/
/
r
/
/
/
/
/
i
-
O.fll 0.05 0. 1 0.7 0.5 I
2C 30 40 50 60 70 80
CUMULATIVE PERCENTAGE
(% Weight
-------
APPENDIX A
RAW TEST DATA
-------
PRELIMINARY VELOCITY TRAVERSE - .- ...
PLANT. LAY ^VJU-...-
DATE' ^ - ^ v--"^
LOCATION -XnWV- -4r-, P^Vซ-'O
STACK I.D.
BAROMETRIC PRESSURE. JR. Hg -."'S
STACK GAUGE PRESSURE, in. H70 - "- ~\
L 1
OPERATORS O'AxV...; 11 1 Me, In >\^,v
TRAVERSE;-
POINT
NUMBER ,
r\/ I 0
,A 1 J
. | ,3^
/ LJ-
/ , -^5"
N
'. '
r* - ' '**A< '.
'V
.^ -.-*""
'AVERAGE
VELOCITY
HEAD
Ups), in.H20
Z3.<#
'Lf\
2 . ฐ
3 f (^
TTT7']
"2,
-------
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
F'LANT
DATE .
SAMPLING LOCATION _-
INSIDE OF FARULLTO
OUTSIDE OF PORT. (DISTANCE A) __Ul_
INSIDE OF NEAR WALL TO x - t '
OUTSIDE OF PORT. (DISTANCE BiTl?
STACK I.D.. (DISTANCE A - DISTANCE Bi -^ '
NEAREST UPSTREAM DISTURBANCE __<3^L"j+-_
NEAREST DOWNSTREAM DISTURBANCE 31
CALCULATOR O'/OoJ / I
SCHEMATIC OF SAMPLING LOCATION
N o-r-c. '
TRAVERSE
POINT
NUMBER
Xv /
1 *
d
y
s
t
! 7
%
7
fo
/#
*z, A,'~, -> 7
FRACTION
OF STACK 1.0.
-'
..-
'
0- /ป 2u.
STACKi.O.
-,.
..
~^ ccxjevcA vnj/
PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1 8 INCH)
\
\ /
\/
A
/ \
/ \
/ \
/ \
/ \
/
,--"
* *
...
"
r
\
DISTANCE B
' ,
\
"\ JO.^-t rj '-' "/ j'\
TRAVERSE p'oiNT LOCATION
FROM OUTSIDE OF PORT
(SUM OF COLUMNS 4 & 5)
* ... -J
':' -' - , '
: ' '
' V
' /' .A:ป '
' v% 1 "
--' ^.. ""*-"-.'*.',
-------
NOMOGRAPH DATA
PLANT
DATE _
SAMPLING LOCATION ^ ^ I 7i-i
CONTROL BOX NO.
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEfviPERATURE i AMBIENT + 20 ฐF). ฐF
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. Hg
(Pmฑ0.073 x STACK GAUGE PRESSURE in in. H20i
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD. in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE ^p. in. H20
^H,5
Tmavg.
Bwo
pm
ps
Ps?
rm
savg.
^avg.
^Pmax.
r/,t
o./
O.A
8.*
13^
Jb*
7-/o
-, ...-4
*- / ซ ^
-T..A
/,o
/75
a. 5
Kb
)'6
3^
i /'
-------
PRELIMINARY VELOCITY TRAVERSE
PLANT__
DATE 1
LOCATION
BAROMETRIC PRESSURE, in. Hg __'i_
STACK GAUGE PRESSURE, in. HoO ..-T---\.-V
QPFRATORS c '/:? .-' -' / '' ' .' /,'..
SCHEMATIC OF TRAVERSE POINT LAYOUT
TRAVERSE
POINT
NUMBER
>' ~ /
i
C-
'J>
V
x
AVERAGE -
VELOCITY
HEAD
Dps), in.H20
X -A
. '79
. <^^
. ^!
i
) -
-!-"
';
-
, 7.<
STACK
TEMPERATURE
v '
/'
TRAVERSE
POINT
NUMBER
v' .''
^^
'1
_. /
AVERAGE
VELOCITY
HEAD
!ApsK in.H20
. . ;< ^
O ")
- 7,;
, //
/
STACK
TEMPERATURE
(Ts). ฐF
/ ? "
-j
/..U
.' --. ~>
-------
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
PLANT ---^ ':j_C_>.:V-.vs--.
DATE . .. "'3 ^ -'. ~".-\
SAMPLING LOCATION >'.. c,.-c
INSIDE OF FAR 'AALL TO
OUTSIDE OF PORT. (DISTANCE Ai._
INSIDE OF NEAR WALL TO
OUTSIDE OF PORT. (DISTANCE B! _
STACK I 0.. (DISTANCE A - DISTANCE 3..
NEAREST UPSTREAM DISTURBANCE
NEAREST DOWNSTREAM-DISTURBANCE._
CALCULATOR sJ.?jy_
-------
NOMOGRAPH DATA
PLANT
DATE. "
SAMPLING LOCATION
CONTROL BOX NO. _
4 V
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20ฐF).ฐF
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. HI
(Prnฑ0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL. NOZZLE DIAMETER, in.
REFERENCE .ip. in. H20,. ' .--
AH,:,
Tmavg.
BWO
Pm
-\'l ;V
ps
Pspm
savg.
^Pavg.
^Pmax.
.9
3/s*
V*
/. t
/ v'0
/ -"i ซC*
/ -""' ,'
>
/o *
-L^.l
30. \
/.o
/*>r
- 7y
. ^/
r*ซ
6>
-------
FIELD DATA
/- - ', '
1 '
1 '
1
j
)
" '.) ..
i i
.(
' f.
i
ji
t;-
, fj:
T
W. .la
t J. t-C-
^ if^oi-
r
ij
.1
*
\
\
\
\
f
>'. >
DATE i t'lc-1 *
SAMPLING L
SAMPLE TYP
RUN NUM3EF
t I OPERATOR _
3CATION 4-'iV. J. fj.
E Pcv-4 >o.l<-^ -
i O/vQ
O'-'Oe,'//
,i/* V"
>..;. .'"ป ' ABSENT TEMPERATURE -VO ฐ r~ . H ซ | } '-'.
TRAVERSE
POINT .
NUMBER
X i
-
^ ' ' ' /
>y
\>-
<!.-.;)
'*
li ?">
\ 1 i. ;
BAROMETRIC
STATIC PRE
FILTER HUM
\. CLOCK TIKE
^v (24 hr
' \CLOCX)
TIME. .Tim X^
~C5 ---ฃฃ/ ^ฃj )
5
/D
D (-
>O
v>' m;iฃ'
vj ';
vi '
KJ
.. 1
' '
PRESSURE 1- *' >1 1
SURE. (P ) * ?-7JL._
",FR (5) --^ '^"/ . t '-\l..^L ''._"-
GAS METER READING
S. (^ T) . / ^ -^
S t ? . ^
<"/CN ,.^ 0
S"7-^-j O'^o
5" ' /5., / ^ o
5 -'/'/. '>
o '7?: 7'2o /--."/
: /' '. '.' <.' :.--
.r ;; <, ,,
jf y~ f
<7 -"/ / r \ Q \ ,
f5 0 >7 . ^ o (9
/,,/;5. 'AtD
(. '(")'/ / f-> T'
(f (jtf . "'. '(' O
/...//. -:> .jo
(;'.> ( "''.. ,/,'. I -'
^.jf'...-,!:'iป
if 1 7,r-'//<-|
to
READ AEiO REC
VELOCITY
HEAD
a . ^ j
- "r ' ";-"' -' .
''. n &ฃ
'/.-;''"''
(O.7,lfl
' .
ORO'ALL DATA EVERY
ORIFICE PRESSURE
DIFFERENTIAL
lilH). in. M20l
DESIREO
CT
C f
r c
: * '
"1 ''"I
. ฃ> '-'
; ;
;'./> //;/: " >
7S;'/l_>y
M. -
'*
I "' "'
i -"' ^
. : ',
, y>
, 5'f
. ^-:;
,--;<
' - -/
- x
, "' ^>
,;v >
ACTUAL
-' ฐ MIMUT
STACK
TEMPERATURE
(TS,."F
\1L{-
/ ^- y
/ <-/ ^
/ '//
/''"
>.',?
'*. '
? Y
C; /
/ /
i / ''
." ,' "-i
%' -'
~ ~FJT/ T-VAT
rr-; p.---
/ "7 :'
OUTLET
*v
,\V)
3 3
i V
. f
i ) \ ;
;-" ...'
. ' - ,
.' i
V" i
f''".-
,-_"". 'f
^ -T
.''i" ' >
<"' '
'v '"''
v" /
*?< V/
/>' -':
'" ' "i
- --' "". - !
' t i
j 1 !
f , .
VP
, '
,
1
1
-. i
' ;":
' .-'.
:!*):
'<!' " ^ _J ' --' ' ' -
"V.c--
s
-------
FIELD DATA
PLANT i ''"..": "-/'--V--'A
DATE '// 'If. 7.'L
SAMPLING LOCATION, Q'->'1
J
'I''"^SAMPLE TYPE.
RUN NUMBER _
OPERATOR
AMBIENT TEMPERATURE _"-1.
BAROHETRIC PRESSURE 7- :?
STATIC PRESSURE. (Ps).. ^- .
FILTER NUMBER is) ,. "-' -\.
PROBE LENGTH AND TYPE j .__:
NOZZLE I.D. _ _^:';6 :-.<-
ASSUMED MOISTURE.".._. /O
SAMPLE BOX NUMBER
METER BOX NUMBER _ { ~ ?.;./ ..
MCHH AH.,. /.-.:/-i;.'.
C FACT OH.!__..;. .;:
PI TOT TUBE FACTOR
REFERENCE Ap .x
NOTE
READ AND RECORD ALL DATA EVERY ._-.._ MINUTES
./ / -J. r;;
TRAVERSE
POINT .
NUMBER
x
!
'
\N CLOCK TIME
SAMPLING \^ CLOC'KI
TKi'E.min "S^
- -^Xฃ/_ฃL
'
//;} S'
GAS MET Eli READING
(Vml. I.3
;,6^ f'.;', {">
VELOCIIY
HEAD
(JipJ. in. H70
i t
- .- i
^
/ ! .'
- ,;
- / ! '. '-
-- ' ' ' '; !
-
IS
/ . . ' ' !
.-/' ' ' . ''
' ' ".' /
f
("* ^j . 1 - V */ '"
....... ._!_-, ,.
, /I"
Lฃ?Lฃ?
';, ,-,-' r-.'i
! ! "-..I I -;_! I..I ! : .1 fj_
-. j / . 't " . r'. M rr-; i
TV': r _ \ ("
"j l".J i'_, j I f
' '-.o ;i..n '-.o ':~...
I ;..'J '. ' "' :-j J ' .!..' :-.i..' :.J I :...i
Ul I"- 'ฃ> CO '-' K.1 !-
1
.... ' >"l
-..
ORIFICE PRESSURE
DIFFERENTIAL
lilHI. in. H,0l
DESIRED 1 ACTUAL
f
.
, '
.16
-,
STACK
TEMPERATURE
|TS)."F
/ "V ' /'
1 -._! \U
i -1 CO OJ
r '.^ j --. ! flj ;""; : r ': ' ;' . \
1 !.'./ '" J' "' -i :-:- C!j Oj ': ("j ' .'!.' '! !
/ i":
DRY GAS METER
TEMPERATURE
INLET
77
-- -; -
..j i-1- '--.I
j'' -I':-- PO
... :
OUTLET
11 -out1'"1
' .- '_ "
' .
i"' :. '
PUMP
VACUUM.
m. Hg
_ . ..: . ._
-
i
0 " i
SAMPLE BOX
ItMPERAIURE.
"'F
IMPINGER
TEMPERATURE.
"F
^ -
j
--
-------
TRAVERSE
POINT.
NUMBER
- / ;
/ /
'
\
i
\, CLOCK TIKE
S^'ป<\^ซ,
1 lint, mm x^
~~~^ -J-L^
.^'
GAS METER READING
'V- "3
..'ป'
' ' !
S-7'3^. 0"
v . . .
:~ ' ' \ v
.,;,- ' ; ;.-'
-, ''-' '< . ' :
/ ." '' ,
- -.
,'
1
' , -J ' ft
s ^,253 ^
VELOCITY
HKAO
iiipsl in H^O
'' /
-V-:
/ ''/,',
^'
-
/
"' '
i
,7iT/
1 ORIFICE PRESSURE
j OIFFEREHTIAL
(4(1). m H^Oi
DESIRED
'' , "}
'.. -;'
""/ ' /
i :
' CV
/
.;
^4
ACTUAL
'
17
i
" r
I
i
... i
i
t
i
.
STftCi^
TEMPERATURE
IT )."F
/?/;
/ 3..'1
,' t\l
/ ..' /
; ' /
'J$
"<"^r -"v
I .31., ,- A'
.
DRY G*
T EMfE
IHLET
'!ซ l "r
111 :ll
^,
'f:
'' I
'i. .9.
... .. _.
kS METER
RATURF.
OUILET
ซซoJar
.._' _-
".:~"
- i
'/, i f
^J -b
.
PUMP
VACliUM
in Hj
:
(
- -
SAMPLE BO/,
HMPERA1URE.
"K
- --...'
!
IMPINGER
TEMPERATURE
ฐF
; .
/ '.
- .
.- > \
< -^
". '.< *~
(
I
-------
FIELD DATA
C
piANTfOX--? ฃy<.ฃ'ry{~- PROQF.IENGTH AND TYPF -.."5' ''"' '''-
TRAVERSE
POINT
NUMBER
i
i *-'
^
, "/.>'
./.Y/''^
" '"'-^
luio
DATE J % IIT-nX \
SAMPLING L
SAMPLE TY?
RUN NUMBEF
OPERATOR
AMBIENT TE
BAROMETRIC
STATIC PRE!
FILTER NUM
' \v CLOCK TIME
. TIME, mm >^
7T~~- il^SL
c,
so
K
-2;.\
}*>
So
3 C"
Va
"7 y
5-3
V'j
1,0
(f:6
-70 "
7v .
&>
i^
ซ/ 0
0 !:>
?.1 :
1 f')^)
I/O
!f4
f^t>
CATION '.T/'//.(f7
F /'////r i /\/\o /'<'' '.-<'
2.
ta&.^.:-_ .
\1PFRATIIRF f / ฐ
PRESSURE ^"/D /
SIIPF. (P ) j? . #
RFR(<;) O ฃ/ ,"-?>?-T"
NOZZLE I.D /J2
ASSUMED KOISTURE-. X-
SAiiiPLE BOX NUMBER
.^
\-/ t o
A
READ AND RECORD AL"b DATfS EVERY
GAS METER READING
(Vm). II3
(2/7. 55 9 ฃ>/&>/
^"^fofyj
^2-2. . i o
^2V, Voi)
ฃ3 Z^/ii" -
^2 ^ 6 <^
/^?O. -/tV.^
H? 3 - o uo
. 6 "5 7. .5^0
' bjt.be*
VELOCITY
' HEAD
(APS). in. H^O
*-, '. .?
L> $ $' 7 *-'' 0 j
4 *--/Qps^
(o i/Jtf"'ฎ
&t-fฃ,otO / (
'" ' ^ A^/'^-V/-
'^^?,-26^
^;5T/. /5o
^53.0^0
. (?ฃ~ฃ,/OP
' /t^y.ioo
(^ ,517.. oVjj
o"(^ / o-^-V.
ORIFICE PRESSURE
DIFFERENTIAL
(dll). in. H20)
PESIRED
,^5.
, 5~-.
s^y ^f
'><&*$ Q.Q >*>*>
' ^^^f .,(,>
' fe5/- 3 5 5 ^X 5? '/
1 ฃ."" ^
ACTUAL
METER 80 X
METER AHj
C FACTOR
5"
/o
!
NUMBER 127 ^
i ' ' ' ' ^ .
/ .:. .-..,-
PITOT TUBE FACTOR
REFERENCE AD b
C^ v ^ MINUT
STACK
TEMPERATURE
(T$|."F
172
f'7&~
{77
I7?
/'/7
X7-7
/7S
i7~(
17' I
r/~z
I7:'
17 H
/ /%
NOTE ..
si' - 0 ' ,-( l-i' '" " 'ill
.- ! S"^^"^-t '
'"" "* ! j^ f" t-'rt'-1-^ v^1-
ES V.r'.;,. -_' ;'
DRYGASfSETER .
TEMPERATURE
INLET
?7
^9
^/Z-
7 ?
92.-.
17 2
-//
v'o
<-;/ .^
9"'^
r//
VV
^ 6
*j?^
K'V
9o
'*/ 0
?/
OUTLET
f S
ฃri
%'x
%ฃ
{~/
O &
ฃ7
-,. c
/ /
/ ' " "^1.673
.1 :' "- x O M'
29.77' 1...P
129.
ij1:. 5 ' "^
"2= y ' '-:"1
1.019
'r ^" = 27395 169 ' '=.
-7 ^- o, f;. o j. '-HJO ii(
,y "J
^/
-3-"'1
5 /C>. *
i . / /) O * / j
/ ('
.- v 1 i
: 3764927979 ' '
= - -' .."..--! i i ! ti.J ' .
i :- j t :: ~= '; .-, S i '-:
.."!. T " " "~ " "' : '-: -:- U h
- ' 0 /.' * "ป
? "7 S 61
- > o 67
-'7ri ^^
v-V 76 j-
C
-------
Lrtlt I ~ J i V-< .- _. - ..
DATE ' - 9/7/7k_
SA?riPLING LOCATION Q(j~f(C
?/.,-* .
SAMPLE TYPE
RUN NUMBER Z:. .^
OPERATOR y.ฃ. {>>.
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSUiiE. |PS) _L~.-'
FILTER NUMBER Isl L_4
~r/~
. ..^_ _
--'i
PK(,'cc LI fiGIH AND TYPE_'rl_lL':';l'ฃ.:.
ป!)//! fid. '/r '&
; -?/_ -.-
-,<.
-
\ ,< 1 ~~> '/
'
: - ."
,.-";.. >
/ '' .' ''
') , ., 1 "i.:^
1
,
!
1
VELOCITY
HEAD
Upjl. '" HjO
',"-' V'*
r / r
-.. - Vr
--.'" '-'
-'
ORIFICE PRESSURE
Olff ERENIIAL
liHI. in. H?0l
OESIREO
' ซL /
ซ /
' L/
s 'V
. vi .-
Y7j JY^i
, 1 ..'. ;
^-
_^15.
- y : <
"Y... - .,--'
j- s
t , ฐ
..? - " !
)
ACIUAL
S1ACK
TEMPERATURE
'"' ';: ':-
1 / '.'
! ....
/ ' ' '
-. _.
1
--' .: . ;
I - .
i
.. .j ._ _7
:::: r.r.i '
D...
3" '-J": !.('"' '-.0 !'' f'--
..:. en c i"i ':o
... ., .. r- !? .i
' - ;~|"; '"'
DRYGASBiETER
1EWP!:.RATURE
INLEF
^ 7
v/
J
1
.. .! o;-
C'..i >l;:l" -
OUTLET
"v~ ;.:;
.-
... /
. -. _
> a, :/:- =:
PUMP
VACUUM.
ill Kg
L.
'
0 '.":- :ป
..,;;, :> a- !.!" .::> T -
0 ::!- 0'-. C'"; * O i;_
r-
SAMi'LE 130 X
U.V.PI RATUHE.
"f
: - -
-i-- -. .,.
". : ," '. , -i : !""l \
IMPINGER
liHf'ERATURE.
"F
-
,*'
. '/
. ' '/
, i
. .'
:/
:, ,-
.,
,
.'
:c '":"'. '."~i ''. '.- ":' o'i S ''::'
-- - t . i ? ." : i
'.
I . C
-------
Y
TRAVERSE
POINT
NUMBER
-,/ -i
\
.
v
"
) :
!
1
\. CLOCK TIME
Sff,LmG \CLOCK,
TIME, mm X^
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NUMBER
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SUMMARY
RECORD OF VISIBLE EMISSIONS
Type oT Plant y 'v
Company f'aire O-: '-<
Plant Address \-
Date
Si
Hours of Observation ~C
Observer __ fi , L _:vv^-c
Type of Discharge''---SjAC
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V/ind Direction __ Hind Velocity '\ Q-T-S rcn'/hr
Plume Description:
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Plunte Dispersion Behavior: Looping Coning Fanning
Lofting Fumigating Othe/
Estimated Distance Plune Visible
-------
RfCORO OK VISIBLE EMISSIONS
Company Nome Qv1-.-, Cy^-Ai vu Date -1 - ' "V - 1 S
Plant Address \Aป v~~ i " --. i v Observer '.*.. (. , ,\-> .- *CfAu
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31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
43
49
50
51
52
53
54
55
55
57
53 '
59
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RECORD OF VISIBLE EMISSIONS
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Observer
Stack Location
Weather Conditions :;>/. v -, .- . . '/ -
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Observer's
^Location
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01
02
03
04
05
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14
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22
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'... Date
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RECORD OF VISIBLE EMISSIONS
Company flame (. )A M '
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Stack Location Vs- ^ '\o
Weather Condi tions : /
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01
02
03
04
05
05
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
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Company Name ---< ^ CWฐ '-"-.
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Stack Location !
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Observer
V.'e cither Condi tions
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31
32
33
3^
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35
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33
39
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30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
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53
54
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RECORD OF VISIBLE EMISSIONS
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01
02
03
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05
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07
08
09
10
11
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14
15
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23
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Observer's
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Date
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-------
APPENDIX B .
LABORATORY REPORTS
-------
ANALYTICAL DATA
PLANT_
DATE <
SAMPLING LOCATION _4-H :
C 1 ' i
SA.MPLE TYPE _l_5::lL'iLL,.lLli
RUN fUJMBLR_._Q;:_L^=.
SAMPLE BOX NUMBER __1
CLEAN UP iMAN.._ !\-'-' '
COMMENTS:
F 'NT HALF
ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
FLASK. FRONT HALF OF FILTER HOLDER
FILTER NUMBER
1 "^ U "7
I -^ ' v* I..
.?
CONTAINER (J-L.
CONTAINER ^.-J....i
LABORATORY .RESULTS
"i """' D i ^
\ , C\ -. ;.'\ rrig
ng
FRONT HALF SUBTOTAL
ffi
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS. CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS. CONNECTORS,
AND BACK HALF OF FILTER HOLDER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER "" '
BACK HALF SUBTOTAL
mg
mg
TOTAL WEIGHT '
Jj^> F ) >, b m&
'
MOISTURE
IMPINGERS ,, f *
FINAL VOLUME _2ฃlฃl_ ml
INITIAL VOLUME ^^ ml
NET VOLUME L.^ *r.,_ ml
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
,
\ ur
f4
I
ItfZ-
TOTAL MOISTURE
SUBTOTAL
-------
ANALYTICAL DATA
PL ANT _ ;._
DATE _... "...,__
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER
SAMPLE BOX NUMBER
CLEAN UP MAN
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
FLASK. FRONT HALF OF FILTER HOLDER
FILTER NUMBER
CONTAINER
CONTAINER l/'U " /
QZLAf
~f, -1F
FRONT HALF SUBTOTAL
LABORATORY RESULTS
X' '.". U.
..) , i . rag
7>
,v r*. /)
M ^."}
.""I
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS. CONNECTORS. AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPiNGERS. CONNECTORS,
AND BACK HALF OF FILTER HOLDER
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
TOTAL WEIGHT
.me
MOISTURE
IMPINGERS
FINAL VOLUME
INITIAL VOLUME
NET VOLUME .
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
ml
ml
ml
17.
TOTAL MOISTURE
SUBTOTAL
-------
ANALYTICAL DATA
PLANT.
DATE_
SAMPLING LOCATION __
SAMPLE TYPE /
RUN NUMBER
SAMPLE BOX NUMBER __ I ____
CLEAN-UP MAN _____ .
<
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE. CYCLONE (BYPASS),
FLASK. FRONT HALF OF FILTER HOLDER
FILTER NUMBER
CONTAINER C<>.
CONTAINER
LABORATORY RESULTS.
FRONT HALF SUBTOTAL
.nig
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS. CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS. CONNECTORS,
AND BACK HALF OF FILTER HOLDER
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
mg
.mg
"""
TOTAL WEIGHT
~> qucr LI
^ ,, ~ f 7^ /
j.
nig
MOISTURE
IMPINGERS
FINAL VOLUME ^!^1
INITIAL VOLUME _
NET VOLUME _
ml
ITll
' S
/rs"'r>
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT _ฃi
NET WEIGHT /J-
SUBTOTAL
TOTAL MOISTURE
-------
ANALYTICAL DATA
PLANT ___.__t^lJ:_:
X
DATE
e
:AJ>-->-
SAMPL1NG LOCATION
SAMPLE TYPE
RUN NUMBER
SAMPLE BOX NUMBER
CLEAN-UP MAN
COMMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE. CYCLONE (BYPASS), CONTAINER
FLASK. FRONT HALF OF FILTER HOLDER
FILTER NUMBER ~2l{?:?~' CONTAINER
LABORATORY RESULTS
FRONT HALF SUBTOTAL
'.. "V ป...W... mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS. CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE 'WASH OF WRINGERS. CONNECTORS,
AND BACK HALF OF FILTER HOLDER
CONTAINER
ETHER-CHLOROFORf/1
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
TOTAL WEIGHT
mg
MOISTURE
IMPINGERS
FINAL VOLUME _.
INITIAL VOLUME
NET VOLUME
SILICA GEL
FINAL WEIGHT _
INITIAL WEIGHT J,
NET WEIGHT _
_
SM
ml
ml
ml
7*
TOTAL MOISTURE.
7"
n
J
SUBTOTAL
-------
ANALYTICAL DATA
PLANT _ - . :-L_lLQ.Lll_._'
DATE _.. "..:-_. : ;
SAMPLING LOCATION ^_-_____
SAMPLE TYPE
RUN NUMBER
SAV.PLE BOX NUMBER
CLEAN UP WAN
COfAMENTS:
FRONT HALF
ACETONE WASH OF NOZZLE. PROBE, CYCLONE (BYPASS).
FLASK. FRONT HALF OF FILTER HOLDER
FILTER NUMBER
'' 5?
t> i 0
t~\
CONTAINER'-
CONTAINER
LABORATORY RESULTS
'', :"N ' < V m g
FRONT HALF SUBTOTAL / Q , r^ ff ^ฃ
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS. CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS. CONNECTORS,
AND BACK HALF OF FILTER HOLDER
CONTAINER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
TOTAL WEIGHT
mg
. mg
MOISTURE
WRINGERS :;; I n
FINAL VOLUME _Zl__l_
INITIAL VOLUME ""? \
NET VOLUME ' ' :"!
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
ml
ml
ml
TOTAL MOISTURE
SUBTOTAL
-------
ANALYTICAL DATA
PLANT_
DATE __. ' . . ..__' ..
SAMPLING LOCATION .
SAMPLE TYPE __
RUN NUMBLfi
SAMPLE BOX NUMBER
CLEAN UP MAN
CO!,"OTS:
ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS). CONTAINER.
FLASK. FRONT HALF OF FILTER HOLDER
---"> -ซ '""* ^
FILTER NUMBER rf Ji'ฑl_l^_ CONTAINER
LABORATORY RESULTS
^ '''', 7
_o.i* I m
FRONT HALF SUBTOTAL Slฐl I > I mg
BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
IMPINGERS. CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS. CONNECTORS.
AND BACK HALF OF FILTER HOLDER
CONTAINER _.
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
-fug
.mg
TOTAL WEIGHT
\
t
m
MOISTURE
WRINGERS
FINAL VOLUME .
INITIAL VOLUME
NET VOLUME .
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
ml
ml
ml
TOTAL MOISTURE
SUBTOTAL
-------
I I
Project No.
' Book No
45
15" 9.5"?^? _!-?-.tt'^' ! 'i*51 ..^fL!^\.,ooj;3._G.<'b
i i i r
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1 i 1 i I 1 M J
i ' T~ i 1 I ' i i
~! i i i i ' ' '
i ' ! TO Pri P '.* Ti'o _
Witnessed & Understood by me.
Dale
*) - 1
Invented by
s
Recorded by
Date,
-------
ฃ/ OO /-/ f <^fv
TITLE
Project No.
Book No.
-------
-------
TITLE
T&A-^j 3-iT-r/i sr:
'reject No.
Book No.
-------
APPENDIX C
SAMPLE CALCULATIONS
-------
SAMPLE CALCULATIONS
Test Run 1 " Ammonium Sulfatc Dryer Baghouse Exhaust Stack
1. Volume of dry gas sampled at standard conditions (63ฐF, 29-92
in. rig) , dscf .
m
(std)
17.647 x Y x V x P, +
m \ b
( T + 460 }
* m i
i 0 69 > 54.94
17.647 x 1.006 x 56.60 x f 29-97 +
\
V , ' \ -3.6 /
vm(std) =
(85-4+ 460
Where:
V / ,v = Volume of gas sample measured by the dry gas meter,
corrected to standard conditions, dscf.
V = Volume of gas sample measured by the dry gas meter at
meter conditions, dcf.
P. = Barometric pressure, in. Hg.
^>H = Average pressure drop across the orifice meter,
in. H20.
T = Average dry gas meter temperature, ฐF.
17-647 - Factor that includes ratio of standard temperature
(528ฐR) to standard pressure (29.92 in. Hg).ฐR/in. Hg.
Y = Dry gas meter calibration factor.
2. Volume of water vapor in the gas sample corrected to standard conditions, scf.
Vw(std) = (0.04707 x V.J + 0.04715
Vw/stdj = (0.04707 x 172 ) + (0.04715 x 14 ) 8.76
Where:
V / ,\ = Volume of water vapor in the gas sample corrected to
standard conditions, scf.
V = Volume of liquid condensed in impingers, ml.
we
-------
- 2 -
W
wsg
0.0^(707
Weight of water vapor collected in silica gel, g.
Factor which includes the density of water
(0.002201 '.'-/ml), the molecular weight of water
(18.0 1b/1b-mole), the ideal gas constant
121.85 (In. Hg} (ft3)/(lb-moie)(ฐR)j ; absolute
temperature at standard conditions (528ฐR), absolute
pressure at standard conditions (29-92 in. Hg), ft /ml
0.0^715
Factor which includes the molecular weight of water
(18.0 Ib/lb-mole), the ideal gas constant
[21.85 (in. Hg)(ft3)/(lb-mole)(ฐR)j . absolute
temperature at standard conditions (528ฐR) , absolute
pressure at standard conditions (23-92 in. Hg), and
A53-6 g/lb, ft3/g.
3. Moisture content.
ws
w
(std)
w(std) m(std)
B
ws
Where:
B
ws
8.76
8.76 + 5k.3k
0.137
Proportion of water vapor, by volume,' in the gas
stream, dimension less.
. Mole fraction of dry gas.
1 - B
ws
M
1 - 0.137 = 0.863
Where:
M .
Mole fraction of dry gas, dimension 1 ess
5. Dry molecular weight of gas stream, Ib/lb-mole.
MW
0.^0(?oC02) + 0.320 (W2) + 0.280
+ % CO)
-------
- 3 -
MWd = (O.VtO x )+ (0.320 x ) +[0.280 ( + )]
28.97 (Air)
Where:
MW, = Dry molecular weight, Ib/lb-mole.
^CO- = Percent carbon dixoide by volume, dry basis.
%0~ = Percent oxygen by volume, dry basis.
'fcNj = Percent nitrogen by volume, dry basis.
%CO = Percent carbon monoxide by volume, dry basis.
O.kkO = Molecular weight of carbon dioxide, divided.by 100.
0.3'20 = Molecular weight of oxygen, divided by 100.
0.280 = Molecular weight of nitrogen or carbon monoxide,
divided by 100.
6. Actual molecular weight of gas stream (wet basis), Ib/lb-mole.
MW = 'MW, x M .') + [18 (1 - M )]
s do' d
MW = (28.97x0.863) + D8 0 -0-863;]
27-46
Where:
MW = Molecular weight of wet gas, Ib/lb-moie.
18 = Molecular weight of water, Ib/lb-mole.
7- Average velocity of gas stream at actual conditions, ft/sec. ,
! s (avg)
85.^9 x C x ( / :.p)
's P av9- x p ZMTT
-------
^qi
85.^9 xO.8^3 x 0.769x "
_ 30.09
= ' ^6.9
V/here :
-,_,- = Average gas stream velocity, ft/sec.
85.A9 " Pitot tube constant, ft/sec X
(ib/lb-moleHm.HgM
. 1"ฐP) (in.' H20)' '_ '
C = Pitot tube coefficient, dimens ion 1 ess .
i, p = Velocity head of stack gas, in FLO.
T = Absolute gas stream temperature, R.
P ' = Absolute gas stack pressure, in. Hg.
8. Average gas stream dry volumetric flow rates, dscf/min.
n 1058.8 x -v x A x M , x P
<*s(std) = -- S- - s -- ^ - ง-
s
1.058.8 x ^6.9 x O.^^9x 0.863x 30.09 '
Mstd) "TTJl + ^i60)
= 980.
Where:
Q / ,N = Volumetric flow rate of dry stack gas, corrected to
standard conditions, dscf/min.
2
A = Cross-sectional area of stack, ft .
1058.8 = Factor which includes standard temperature (528ฐR) ,
standard pressure (29-92 in. Hg) , and 60 sec/min,
(ฐR) (sec)
(in. Hg) (min)
9- Isokinetic variation calculated from intermediate values, percent.
-------
- 5 -
17-316 x T x V
m(stdj
2
V x 6 x P x M , x (D )
s s d n
I = 17.316 x 531 x 5^.94
~wTs x fio x 30.09" O63x( o. 189 )2
107.8
Where:
I = Percent of isokinetic sampling.
Q = Total sampling time, minutes.
D = Diameter of nozzle, inches.
17-316 = Factor which includes standard temperature (528ฐR) ,
standard pressure (29-92 in. Hq), the formula for
calculating area of circle 1"^ D . -
r , conversion of
square feet to square inches ( 1^'0, conversion of
seconds to minutes (60), and conversion to
percent (100), (in. Hg) (in2) (min) .
(ฐR) (ft2) (sec)
10. Particulate concentration, gr/dscf.
C] = 0.015^32 x M
m(std)
C = 0.015^32 x ^^ = 0-028
1 5^.9^
Where:
C, = Particulate. concentration, gr/dscf.
M = Total weight of particulate caught by train, mg.
0.015't32 . = Conversion factor of gr/mg.
11. Particulate mass emission rate, Ib/hr.
PMRt = 0.00857^ x C1 x Qs(std)
0.0085714 x 0.028 x 980 = 0.24
-------
- 6 -
Where:
PMR = Particulate mass emission rate, Ib/hr.
0.008571A = Conversion factor relating minutes to hours (60), and
grains to pounds (7,000).(lb) (n>in)/(gr) (hr) .
-------
APPENDIX D
EQUIPMENT CALIBRATION DATA
-------
;c r " .^
s/t--. i-
Da te
Barometric pressure,
Box Hn
.in. tig Dry gas meter !lo. 1
Or i f ice
manonie tcr
setting ,
All,
in. 1(20
0.5
1.0
2.0
Z^rtf
1-Sjxtf'
8.0
Gas volume
wet test
meter
vw.
5. cos
xSVaCG.
xrv*?.i
/ ซ "' ' V
^n" T J .^ i/ '. &?
10
Gas volume
dry gas
meter
S-041
J- 7ฃ
/O/.O
/33f0
Time
0,
mi n
njl.
'7.65C
13, /U
1.15s
7C-V5b
Average
Y
,?7Y<
AllQ
/ '^>?"t
/.?2SJ /,7/? 7
/.ocj A8?*ป
/.co 6
,r/-?^
/1006
/,905
/. 7 r-?
/,77fe
Ca1cula t ions
All
0.5
1.0
2.0
f^rCT
8.0
AM
1176
0.0360
0.0737
0.147
0.294
0.431
0.503
Y
Vw Pb (td + 460)
V^(pb + iirs) (tw+ 46ฐ)
,IILB
0.0317 All f(tw ^ 460) el 2
Pb (td -i- 460) 1 V 1
u w L_ W J
Y = Ratio of accuracy of wet test meter to dry test meter. Tolerance = ฑ 0.01
= Orifice pressure differential that gives 0.75 cfm of air at 70ฐ F and 29.92
inches of mercury, in. I^O. Tolerance - - 0.15
-------
,s
-- .002.
Date
Box Mo.
Barometric pressure, Pb = in. llg Drv gas meter ilo. ff/Vj?/
U
Or i f ice
manometer
setting ,
AH,
in. H20
0.5
1.0
2.0
'5.0
,S>rCr
8.0
Gas volume
wet test
meter
V
S.ooo
Xitftft
1 0 * @Qj
] Q , C 0 0
-Mf.oot
10
Gas volume
dry gas
meter
// (9 f?
I0,5k(
s.^.^
Tempera ture
Wet test
Meter
ฐF
7^^l_j
7// 7-tLj
7-f _22
73 _
73 73
Dry gas
Inlet
ฐF
'7Z.
xlฃl
^3
jH^
/D 2-
Outlet
ฐF
70
^Z
rTfr
Vfjf
*%&.
fiie ter
Average
ฐF
H.o
?y,7ฃ>
gฃj>
96.2^
Time
0,
min
/?.6^
#2^
i?,W'j?
?.?&
^5" IT! 5^3
Average
Y
/.^r
8.0
AH
1576
0.0360
0.0737
0.147
0.29-1
0.431
0.503
Y
Vw Pb (td + 460)
vd(pb + rf-e) (*ซ + 46ฐ)
AH@
0.0317 AH f(tw + 460) el 2
7bTtd~~46o) [~"v; -J
y = Ratio of accuracy of wet test meter to dry test meter. Tolerance = i 0.01
h'g = Orifice pressure differential that gives 0.75 cfm of air at 70ฐ F and 29.92
inches of mercury, in. I^O. Tolerance - i 0.15
-------
Date
Box No.
Barometric pressure,
in. Hg
Dry gas meter Do.
Ori f ice
manometer
setting ,
ill.
in. M20
0.5
1.0
2.0
4.0
6.0
8.0
Gas volume
wet test
meter
V
5
5.0^0
10
10
10
Gos volume
dry gas
meter
f ^3
7 ซ./ / ,* i t "C
t it
/ / . , .
i
Temperature
Wet test
Meter
ฐF
7 ฐ "> 6
70 7ฐ
~> (i
. u
Dry gas
Inlet
d i *
ฐF
^\\_
';iv
"->,
Outlet
ฐF
5C^/^_
^ "*^r- /
'~'~S.' ,.
meter
Average
ฐF
eo-c
5S.S
^rj.
^7!
Time
o,
mi n
0^
1C3^
Y
3
1,01
I3,6~?iuo6
9 /==/:
Average
(.Do
\ ^ *\
fe 'U 'sJs
3 ^ ,03
4- <3u 1 ฃ
1^ t
Calcula tions
AH
0.5
1.0
2.0
4.0
6.0
8.0
AH
ITTe
0.0360
0.0737
0.147
0.294
0.431
0.588
Y
Vw Pjj (tj ป 460)
^ + rare) (^ + 46ฐ)
AH,
0.0317 AH f(tw + 460) el 2
Pb (td + 460) [ vw J
= Ratio of accuracy of wet test meter to dry test meter. Tolerance = ฑ 0.01
= Orifice pressure differential that gives 0.75 cfm of air at 70ฐ F and 29.92
inches of mercury, in. f^O. Tolerance - ฑ 0.15
-------
O
Date_
3,0, Q
Barometric pressure, PL = in. llg
Box No.
Dry gas meter Mo.
Calculations
Orifice
manometer
setting ,
All.
in. H20
0.5
4-^,5
-5-rsaS
4.0
6.0
8.0
Gas volume
we t tes t
meter
v.'m
5
' lf''%^
44- S
AM';10
10
10
Gas volume
dry gas
meter
V
7/t,.O^5"
to i . nz$
> i /i
o%' ; . AS 7
Wet test
Meter
ฐF
/cHvo
Tenipe
i)
Inlet
d i *
ฐF
^?
7V
?~~^.
-a ture
ry gas
Outlet
ฐF
?r~
^ i
*^~rj
me ter
Average
"F
A-'./r
* i f
' ' *, ; ^.-:
Average
Time
0,
min
13 ^^r
3 C^(J !>,>
i/3 .ฃ3
A7S7-
Y
l,^
t.oi^
Uf*
|.6\
All
' i -S3
_J Ji^
5 i^Jt
W 1.8^,
AH
0.5
1.0
2.0
4.0
6.0
8.0
AH
1376
0.0360 '
0.0737
0.147
0.294
0.431
0.508
Y
Vw Pb (^ + ^0)
Vd(Pb + f576j (tw + 460J ;.
-
A 11(3
0.0317 All -f(tw 4 460) e] 2
Pb (td + ^60} [ Vw
1
i
,Y = Ratio of accuracy of wet test meter to dry test meter. Tolerance = ฑ 0.01
= Orifice pressure differential that gives 0.75 cfm of air at 70ฐ F and 29.92
inches of mercury, in. f^O. Tolerance - - 0.1T>
-------
Date..
Barometric pressure,
in. llg
Box Ho.
Dry gas meter ilo.
Or i f ice
manometer
setting ,
Ail.
in. !I20
0.5
1.0
2.0
4.0
6.0
3.0
Gas volume
wet test
meter
vw.
ft3
5
5,
10
10
10
Gas volume
dry gas
meter
vd
ft3
IlfJ&a
pii5"^
'-Trr.'/"^?
10 |
Temperature
Wet test
Meter
wป
ฐF
7V
7V
?v >v
D
Inlet
(J 1 *
ฐF
3^
*'^V.
i! C
ry gas
On 1 1 e t
t-do '
ฐF
^ J
T6 ^
^6/C
me ter
Average
t(J
ฐF
sy
T ime
0,
m i n
&3S
j? ? I0?//]
.^C7
i&i's
Y
AHp
/.^ 1*11
/.ocg 7,83
^.T
~ '1
Average / t*-*)^ /'
"ฃ ( .^fT
X N ซ^-
\ . o ^>
Calculat ions
AH
0.5
1.0
2.0
4.0
fi.O
8.0
;
All
1376
0.0360
0.0737
0.147
0.294
0.431
0.508
Y
Vw Pb (*d 4 <160)
Vd.(Pb - nIJ-6) (tw + 460)
>
aii(3
0.0317 All [{t,.. -f 460) el 2
PbTt d~~4 6 6 ) [ V~ _
Y = Ratio oY accuracy of wet test meter to dry test meter-. Tolerance = ฑ 0.01
= Orifice pressure., differential that gives 0.75 cfm of air at 70ฐ F and 29.92
inches of mercury, in. J.^O. To'lerance - ฑ 0.15
-------
Date.
Barometric pressure,
in. Hg
Box No.
Dry gas meter No.
0.7
Or i f ice
manometer
setting ,
ill,
in. II20
HJ^S-
4UL
2.0
4.0
6.0
8.0
Gas volume
wet test
meter
V
5
5
10
10
10
10
Gas volume
dry gas
meter
~s ,- "/ r* " .
'./ -; '
Wet test
Meter
ฐF
/ * /-
^V ->v
Tempe
D
Inlet
ฐF
GC'J
a Lure
ry gas
Ou t 1 e t
ฐF
c l5N'j>
AC
meter
Avo'"a ge
tt|,
ฐF
"5 < !
//
T ime
0,
m i n
'0.1'
/0,?o
..
V
A CปC
/roc?
ซ '.77
c, i . Tl
"
.
Average
Calcula t ions
AH
0.5
1.0
2.0
4.0
6.0
8.0
A It
AH
13.6
0.0360
0.0737
0.147
0.294
0.131
0.508
Y
Vw Pb (fcd 4 ^0)
ii /n i -i' 1 /t L /^nl
V4Pb + 13767 (tw + 460J
Al!|3
0.0317 AH Rt,. -f 460) 8] 2
1
/ 4 -\ \ 1
Pb (tcj 4 -IbO) L VW J
= Ratio of accuracy of wet test meter to dry test meter. Tolerance = * 0.0)
= Orifice pressure differential that gives 0.75 cfm of air at 70ฐ F and 29.92
inches of mercury, in. HjO. Tolerance - - 0.15
-------
R Y \-> V_. v
CH.KD BY
PROJECT
SUBJECT
J 0 A TF ^
DATF
P ; Vo i:
I 2- ( / / .JrJT
T^ W <
H"^ ^^_j/ .*ป^ซ.t ^,~%V* >
v_-s. \\ Vo r -5.-
rlSHFFT OF
WO NO
V\o- "f-^c.'to^S
0.
V
.S^o .21,1
T
VJ
-------
APPENDIX E
DETAILED BAGHOUSE INFORMATION
-------
xc.v.er.tai Chemical Company
September 27, 1978
Mr. Berry Jackson
Ray F. Western, Inc.
West on Way
Westchester, Penn. 19330
Dear Sir:
There were 17 tons per hour produced on the 12 and 13th.
Enclosed are the production and spec sheets your requested.
Please return the spec sheets.
Thank you.
Sincerely yours ,
OCCIDENTAL CHEMICAL COMPANY
cu-i
R.E. Kleissle
Production Manager
9802 Lawndale P. 0. Box 5337 Houston, Texas 77012 (713) 477-8811
-------
HOUSTON SULFATc
Tons
Srorf -
O
Finish -
Tofal -
SPARGER PRESS: High ,^_T
Low
Flushing Every
10 12 14 16 18 20 23 F
;ed ch AM AM PM PM
3
/6
A'
/->
,~
.
Ton 5
Start -
SPARGER PRESS: 'High ::
Finish - /^ 7'
LOW
Toi-a! ~ /
PJB:._.._Avorpge; ^7. -Q J.P.H.
Flushing Every
8 10 12 14 16 18 20 28 F
ked af: AM AM PM PM
/
'3
'3
'1
/j>
_--
>*?
a^?
/ ^;
I d ? ^
Tons
Srarf -
Finish -
Total -
Average: / 7, q T.P.H.
SPARGER PRESS: High
Losv
8 10 12 14 16
20 28 F
CHeckocI ah AM AM PM PM
u
li
fa
.-^
^
/^_
/'-L
//
/"
Tons
THIS MONTH:
Tons
AVERAGE
T.P.H,
Y.T.D.
Tons
-------
DATE:
HOUSTON SULFATE
\m
; V
Start -
SPARGER PRESS: High
Finish-
Tons
Lov/
MffRKS: Average: //? 2_ T.P.H.
--1 r-r
ฃ^_/._
Flushing Every ^
8 10 12 14 16 18 20 28 F
^checked ct: AM AM PM PM
ซ! ,.. ..,,_T1.__T^ , r - . .
/
If
//
/ป-
/s-
-
/?/-
if 2
u?i:- .
X ^
/ ^/O, & Tons
Start - (0
Finish - /--C/O /$//
Total - /--/. 0 ,vj^/
ฃฃ"
SPARGER PRESS:
Flushing Every
High s-?
Low ^
6
/
^
T P'H
8 10 12 14 16 18 20 28 F
Oil- checked at: AM
AM
PM
PM
//
/: x-:
HI FT 3 '*j^J>?'..?J...<^ f-^.
E.fijปRKS: Average: ///7 T.P.H.
Start -
_F_m?sh.- JH, / tf .?,
Total - /i/ / ^ -7.
?*'
SPARGER PRESS: High
Low
Flushing Every
8 10 12 14 16 18 20 28 F
|งl Checked at: AM AM PM PM
2
;z.
o
/7
/T
_
i*
13
A^TY TOTAL: V,^. t/ Tons
JtH 2URt-.Y AVERAGE
THIS MONTH:
/ / 7
Tons
T.P.H.
Y.T.D.
Tons
-------
APPENDIX F
PROJECT PARTICIPANTS
-------
PROJECT PARTICIPANTS
The follov/ing Weston employees participated in this project:
Peter J. Marks
Laboratory Manager
econENVIRONomics Division
Barry L. Jackson
Supervisor,. Air Testing
Jeffrey D. O'Nei11
Project Scientist Assistant
econENVIRONomics Division
econENVIROMomics Division
Gregory Celi ano
Assistant Project Scientist
econENVIRONomi cs D i v i s i on
Richard J, Urban
Laboratory Technician
econENVIRONomics .Division
David D. Maloney
Laboratory Technician
econENVIRONomics Division
-------
\,v
cer
tifies tnat
&\RRY L, JACKSON
ia6 completed
VISIBLE EMISSIONS EVALUATION SEMINAR
Date:
T. ftl
.' 71
Dale:
DIRECTOR, CENTER FOR AIR
ENVIRONMENT STUDIES
Recertified:
Date:
VICE PRESIDENT FOR
CONTINUING EDUCATION
------- |