United  States
Environmental Protection
Agency
                                             Air
                                                                                      Office of Air Quality
                                                                                      Planning and  Standards
                                                                                      Research Triangle Park'NC 27711
EMB Report  78-NHF-2
February  1970
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                      SOURCE EMISSIONS TEST REPORT

                       OCCIDENTAL CHEMICAL COMPANY
                            Houston, Texas
            AMMONIUM SULFATE  DRYER  BAGHOUSE EXHAUST STACK
                                             Barry L.  Jackson
                                             Supervi sor
                                             Ai r Test i ng
RFW W.O.  #0300-81-04
Contract No.  68-02-2816
Work Assignment  No.  2
                                                              JU
                                             Peter J.  Marks
                                             Department Manager
                                             Laboratory Services

                                             for:  ROY F.  WESTON
                              Prepared by:

                             ROY  F. WESTON
                   ENVIRONMENTAL  CONSULTANTS-DESIGNERS
                              Weston Way
                    West  Chester, Pennsylvania 19380
                                  692-3030

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                                                        TABLE  OF CONTENTS


                                                                     PAGE

LIST OF TABLES AND FIGURES                                             i

SUMMARY                                                                1

INTRODUCTION                                                           3

DESCRIPTION OF PROCESS                                                 5

DESCRIPTION OF TEST LOCATIONS                                          7

   Ammonium Sulfate Dryer Baghouse Inlet Duct                      .    7
   Ammonium Sulfate Dryer Baghouse Exhaust Stack                       7

DESCRIPTION OF SAMPLING TRAINS                                        10

   Particulate Sampling Trains                                        10
   Particle Sizing Train                                              11

TEST PROCEDURES                                                       14

   Preliminary Tests                                                  1iป
   Ammonium Sulfate Dryer Baghouse Inlet Duct                         1^
   Ammonium Sulfate Dryer Baghouse Exhaust Stack                      15

ANALYTICAL PROCEDURES                                            '     .16

   Particulate Sample Recovery                                        16
   Particulate Analyses                                               16
   Particle Size Sample Recovery and Analyses                         17

DISCUSSION OF TEST RESULTS                                            18

APPENDIX A  -  Raw Test Data

APPENDIX B  -  Laboratory Reports

APPENDIX C  -  Sample Calculations

APPENDIX D  -  Equipment Calibration Data

APPENDIX E  -  Detailed Baghouse Information

APPENDIX F  -  Project Participants

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TABLE
 NO.

  1
     TITLE

Ammoniurn .Sulfate Dryer Inlet Duct
Summary of Test Data

Ammonium Sulfate Dryer Exhuast Stack
Summary of Test Data

Ammonium Sulfate Dryer Inlet Duct
Summary of Test Results

Ammonium Sulfate Dryer Exhuast Stack
Summary of Test Results
LIST OF TABLES AND FIGURES

                      PAGE

                        20


                        21


                        22


                        23
FIGURE
  NO.

  1

  2
     TITLE

Ajrimon i urn Sul fate Dryer and Baghouse

Ammonium Sulfate Dryer Baghouse Inlet Duct
Port and Sampling Point Locations

Ammonium Sulfate Dryer Baghouse Exhaust Stack
Port and Sampling Point Locations

Particulate Sampling Train
EPA Method 5
Baghouse Inlet Duct

Particulate Sampling Train
EPA Method 5
Baghcuse Exhaust Stack

Ammonium Sulfate Dryer Baghouse Inlet Duct
Particle Size Distribution
                      PAGE

                        6

                        8
                                                                               12
                                                                               13

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                                                   SUMMARY

The Emission Measurement Branch of the U.  S.  Environmental Protection
Agency contracted Roy F. Weston, Inc. to conduct a source testing and
analysis program at Occidental Chemical  Company's Houston, Texas
Ammonium Sulfate Plant.
The primary objective of the testing program was to quantify the
participate emissions to the atmosphere from the Ammonium Sulfate
Dryer Baghouse Stack.  This objective was achieved by performing a
series of three particulate tests utilizing EPA Method 5    procedures
at the baghouse exhaust stack location.  In addition, visual determinations
of plume opacities were made simultaneously with each particulate test at
                                                    (2)
the source discharge point according to EPA Method 9    protocol.  Also,
EPA Method 5    particulate tests were executed at the baghouse inlet
site simultaneously with the exhaust stack tests to measure the potential
uncontrolled emissions and to calculate particulate removal efficiencies.
                   n
A singular Anderson  cascade impactor test was conducted at the baghouse
inlet location to determine the particle size distribution of the
entering particulate matter.
The particulate matter emission results are summarized below:
                     Ammonium Sulfate Dryer Baghouse
                                          Particulate Concentration
                                         Grains/DSCF     Pounds/Hour
Test
No.
1
2
3
Date
9/12/78
9/12/78
9/12/78
9/12/78
9/13/78
9/13/78
Test
Locat ion
Inlet Duct
Exhaust Stack
Inlet Duct
Exhaust Stack
Inlet Duct
Exhaust Stack
1.01
0.028
0.96
0.085
3-83
0.093
8.36
0.24
7.84
0.70
31.2
0.74
Part iculat
Removal
Eff i ci ency
Percent	

  97.2
                                                                              91.1
                                                                              97-6
 ^  'Code of Federal  Regulations,  Title  kQ,  Part  60, Appendix  A,  "Standards  of
    Performance for  New Stationary  Sources,"  August 18,  1977-
 (^Federal  Register,  Vol.  39,  No.  219,  November 12,  1974.
 (3)0p.  Cit.

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No visible emissions were observed emanating from the baghouse exhaust
stack during the test program by the certified observer.

Figure 6 illustrates the particle size distribution of the particulate
matter at  the baghouse inlet location.

Detailed summaries of test data and test results are presented in
Tables 1 through 4 of this report.
                                 - 2 -

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                                                        INTRODUCTION

The Emission Measurement Branch of the U. S. Environmental Protection
Agency contracted Roy F. Western,  Inc. to conduct a  source testing and
analysis program at Occidental Chemical Company's Houston, Texas
Ammonium Sulfate Plant.- The objective of the testing program was to
measure various emission parameters from Oxychem's Ammonium Sulfate
Dryer.

The location tested, plus the number and types of tests performed at
each site are listed below:

     1.  Ammonium Sulfate Dryer Baghouse Inlet Quct.
         a.  Three particulate tests by EPA Method 5-
         b.  One particle size distribution tes-t by cascade
                                D
             impaction  (Anderson  ).
     2.  Ammonium .Sulfate Dryer Baghouse Exhaust Stack.
         a.  Three particulate tests by EPA Method 5>  Each
             particulate test .was performed simultaneously
             with one of the  inlet duct tests.
         b.  .Three opacity tests  by EPA Method 9-  Visual
             determinations of plume opacities determined
             concurrently with the particulate tests.

All tests were conducted during the period 12-13 September 1978 by Weston
personnel and were observed by Mr. Dennis P. Holzschun, EPA Technical
Manager.

Test data and test results are presented in Tables 1 through k of this
report.  Particle size  distribution results are shown in Figure 6.  Also
incorporated herein is  a description of the test locations, test equipment,
test procedures, sample" recovery, and analytical methods used during the
                                 - 3 -

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test program.   Raw test data,  laboratory reports,  sample calculations,
equipment calibration data, baghouse details, and  a list of project
participants are provided in Appendices A through  F,  respectively.

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 III.  PROCESS DESCRIPTION AMD OPERATION



       The: Occidental Chemi-ca'l plant produces  ammonium sulfate (AS)  from ammonia



 and sulfun'c acid.  ATI of the AS produced is sold for use as a fertilizer.   The



 plant, did not operato continuously during 1978 due to problems  with sulfuric



 acid supply and cyclical  market conditions for AS.



 A.     Process Description



       Su "If uric acid and ammonia are combined  in a crystal Vizer or saturator.



 The reaction in the saturator to form the AS  occurs with  much evolution of



.heat.  The reaction takes place in a medium.of "mother liquor"'which is a dilute  •



 solution of AS.  As the reaction proceeds and the concentration of AS in the



 ir.other liquor increases,  the solution becomes supersaturated, and the AS   /  '•";.•



 begins to precipitate in  the form of crystals.   The crystals  grow to about



 1/8" diameter maximum and leave the saturator through bottom  feed lines to



 centrifuges,  A slight, vacuum (ll.O psia) is  maintained on the saturator



 to aid evaporation.



       At the centrifuges, the crystals are separated from the mother liquor



 and are discharged as wet crystals onto a conveyor belt "leading to  the



 dryer.  The mother liquor goes back to storage.  The wet  crystals contain



 about 2 to 3 percent moisture at this point.



       The dryer installed at this plant is a  natural gas,  direct-fired rotary



 drum unit.  The water content of the AS is reduced to a range of about



 0.3 percent, to 0.5 percent.  Some drying of AS also occurs on the lengthy



 conveyor belt feeding the dryer.  From the dryer the AS passes  to a screening



 operation where "granular" and "coarse" products are separated.

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      The baghouse is  a Carter Day  unit  Model  Mo. 24RV60 containing ?•>?.() square



 feet of dacron felt cloth.   It employs  a  periodic reverse jet of filtered



 air to  clean  the bags.    The AS collected drops into a conical  bottom in



 the housing and is  pumped back,  to the  mother liquor tank after res'lurrying.



 The bags  in the baghousc had  been  replaced.during the week of September 4,



 prior to  the  test.




      A  schematic diagram of  the  dryer and baghouse is presented in Figure 1.



 B.    Process  Operation



      The  purpose of the test  program was  to measure emission levels  from



 the Occiden.tal. Chemical baghouse controlling the dryer.  Process conditions



 were  carefully observed and  testing was performed only during periods when



 the plant was  operating normally.  During the tests, pertinent operating



 conditions were monitored and recorded  on process data sheets.  This  data is



 summarized in  Tables  I-IV of Appendix B.



      The  plant was  operating  over  90 percent of its design capacity during



 each  of the three emission tests which  were conducted.  No calibrated weigh



 belts were used at  this plant.   The production rate was determined most



 accurately by  a digital sulfuric acid flow meter which registered the total



.acid  withdrawn from storage  for  a  24-hour period.  The plant reported to be



 operating with 94 •- 95  percent I-LSCL.



      The  temperature  of the  exit gases  from the dryer were read off a strip



 chart in  the  control  room.   Temperatures of this strip chart were slightly



 lower than those measured by  the test team at the baghouse inlet.  The temperature



 and the centrifuge  motor drive amperage were monitored during the emission tests



 to  establish  the steady state operation of the dryer throughput rate.  Other



 process parameters  monitored  are. included in Appendix B. Tables I-IV.

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      The -Pollowing parameters were monitored during the tests to verify



that the dryer was operating normally,





      1.  Acid flow rate and totalizer amount,



      2.  Ammonia flow rate.



      3.  Dryer outlet gas temperature.



      4.  Centrifuge amperes.



      5.  Temperature of the vapor leaving the saturator,.



      6.  Liquid level in the saturator (inverse reading).



     "7.  Liquid level in'the mother liquor tank".



      8.  Neutral point titration (ml of O.'IM NaOH).



      9.  Percent, solids in  -the magma.





      The raw data sheets for these parameters are included  in .-./•....' .



Table* I - IV.



      Process monitoring for test No. 1 began at 9:50 a.m.  on September 12,



1978, and continued until 12:35 p.m.  The centrifuges were  shut down for



20 minutes for water flushing of the centrifuge inlet lines.  The AS



production ceased during this period but the acid and ammonia feed to the



saturator continued.  Since  the production rate obviously affected emissions,



the  test team was advised immediately when the production stopped.  Emission



sampling was stopped for the 20 minute period and resumed after a short



period  to allow buildup of AS in the dryer.

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    •Monitoring for test Mo.  2 began  at 1 r/l.O  p.m.  on  September 12, 1978ป



and concluded at 4:20 p.m.   Test No.  3 process  monitoring began at 9:H> a.m.



on September 13, "1978, and  concluded  at 1:00  p.m.   As with the first tests,



the emission sampling was suspended during  centrifuge servicing.

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                         OCCIDENTAL  CHEMICAL  COMPANY
                             Houston,  Texas

                                FIGURE 1

                   AMMONIUM SULFATE  DRYER AND BAGHOUSE
                                                  Gas  Flow to Atmosphere
                                                             A
                                          Exhaust Stack—ฃ
                                          Test Site
                              Inlet Duct
                              Test Site
                     Ammon i urn
                      Sul.fate
                       Dryer
Shelter
                                                      r
                                                              4 7
                                                                           Baghouse
                                                                           Fan
                                                                         Product
                                  - 6 -

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                               TABLE I

                 SUMMARY OF AS PRODUCTION RATE DATA
Test; No. 1
Average indicated acid rate, gpm
Standard Deviation, gpm
Equivalent AS production rate, Tons/hr ,
based, on .indicated acid rate
Acid rate from, totalizer, gpm
Equivalent AS production rate, Tons'/hr,
based on acid totalizer rate
Ammonia Rate, Ib/hr (average readout,
t e iTip er a t u r e c o r r e c t e d )
Standard Deviation, Ibs/hr
Equivalent: AS production rate, Tons/hr ,
based on ammonia rate
Ibs
A.S product 'conveyer sample • rate,-— — -
1
31.67
.38

19 .. 1
28.8

17,4

8400
141

16 . 3
4.32
2
31.8
Small

17.6
29.0

16 . 4

8402
Small

16.3
3.90
3
34 .
Small

19.4
34.1

.20.6

843S
Small
r'
16.4
3.81
Equivalent AS production rate,Tons/hr,.
  bas&u on AS product conveyor rate          18.7     16.9     16,6

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                              TABLE  II
      ADDITIONAL PROCESS PARAMETERS MONITORED  DURING  TEST  NO.  1
Elapsed Time, ruin..

Sciturator Vapor Temp,  F

Dryer Exit Air Temp,  F

Percent Solids in the magma

Neutral Point Titration,
  ml 0.1N NaOH


Centrifuge Current,  Ampsres

Unit: #2
                                      0     30     60     90    120    1/sO

                                     182   182   182    182   '181    182

                                     135     -•    135     -     135    135

                                      70           70     •      74     72
                                     8.0
           6.0
           8.2 .  12.0
                                     20
            18
            18    18
Unit v:3
18
23
                                                              25    25

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                              TABLE III
     ADDITIONAL PROCESS PARAMETERS MONITORED DURING  TEST  NO.  2
Elapsed Time, rain.

S.o.turator Vapor Temp, F

Dryer Exit Air Temp, ฐF

Percant Solids in magma

Keutral Point Titration,
  ir.l 0..1N NaOH .
  0    30    60    90  ' 120   150

182   183   183   183   183   183

136    •-    136    -    138   136

 71    71    70    72    .71    7.1


7.8   7.8   7.8   7.8   7.8   7.8
Centrifuge Current, Ampere?

Unit ฃ2

Unit i/3
       20

       23
20

23
18

22
18

22
18

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                               TABLE IV
      ADDITIONAL  PROCESS  PARAMETERS MONITORED DURING TEST NO. 3
Elapsed Time:, mia.

Sa&urator Vapor Te.inp,  F

Dry-ar Exit Air Teran,  F

Percent Solids in magma

Neutral Point Titration.
  nil OV1N NaOH
  0    30    60    90   120    150

182   182   182   182   182    183

136   . -    135    -    136    138

 71    71    70    70     71     71
7.8   10.0
           4.8   6.8    7.8
Centrifuge Current, Arr.pferes

Unit #2

Unit ฃ3
 20

 22
21 .   23     6'-..   0     18

25    25    25    25      0-
*Shut.down - Unit No. 1 operating but ammeter was  defective

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                                                   DESCRIPTION OF TEST LOCATIONS
Ammonium Sulfate Dryer Baghouse Inlet Duct

Two 3" I-D.  test ports approximately 90  apart were installed on a
straight section of the 11" I.D.  stack at a location  which v/as 5-0
stack diameters downstream and 2.3 diameters upstream from the
nearest gas  stream flow disturbances.  EPA Method 1 ^   criteria for
this test location required a minimum of 20 traverse  points but due
to a heavy build-up of particulate matter cover ing -^68% of the
inside area  of the duct the particulate tests were run at a single
point of average velocity during  each of the three test runs.  See
Figure 2 for port and sampling point locations.

Ammoniurn Su1 fate Dryer Baghouse Exhaust Stack

Two 3" I.D.  test ports were placed on one side of the 7-1/2" x 8-5/8"
rectangular  exhaust stack serving the baghouse.  The  ports were located
15 diameters downstream and 10 diameters upstream from the nearest flow
disturbances.   Since the eight and two diameter criterion were met, a
minimum of eight traverse points  were required by EPA Method 1
regulations.   Figure 3 illustrates duct geometry plus port and sampling
point locations.
                                 - 7 -
        of Federal Regulations, Title ^0, Part 60, Appendix A, "Standards
   of Performance for New Stationary Sources," August 18, 1977-

-------
 Baghouse
Port X
                                FIGURE 2

                       OCCIDENTAL CHEMICAL COMPANY

                             Houston,  Texas

               AMMONIUM SULFATE DRYER  BAGHOUSE INLET DUCT
                    PORT AND SAMPLING  POINT LOCATIONS
                                                                                  Roof
                                                             Ammonium Sulfats
                                                                   Dryer
                       Port Y
Blockage
                Duct Cross-Sectional  View
                                 - 8 -

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                 OCCIDENTAL CHEMICAL COMPANY

                      Houston, Texas


                         FIGURE 3


        AMMONIUM  SULFATE  DRYER BAGHOUSE EXHAUST STACK
r










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2
3
iป
Distance From
Inside Near
Wai 1 , Inches
1
2-3/4
A-5/8
6-1/2
                                                            oo
                                                               FAN
                                                                        7-5'
                                                   METAL STACK

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                                              DESCRIPTION OF SAMPLING TRAINS

Parti culate Sampling Trains

The test train utilized for participate sampling at the bag house inlet duct
location v/as the standard EPA Method Five Train (see Figure *<) .

A stainless steel nozzle was attached to a heated (.-^250 F) 3'  borosilicate glass
probe which was connected directly to a borosilicate filter holder containing a
4" Reeve Angel 900 AF glass fiber filter.  The filter holder v/as maintained at
                 o                                                 R
approximately 250 F in a heated chamber, and was connected by Tygon  vacuum
tubing to the first of four Greenburg-Smith impingers which were included in
the train to condense the moisture in the gas stream.  Each of the first two
impingers contained 100 ml of distilled water, the third was dry and the final
impinger contained 200 grams of dry pre-weighed silica gel.  The first, third,
and fourth impingers were modified Greenburg-Smith type; the second was a standard,
Greenburg-Smith  impinger.  All impingers were maintained in a crushed ice bath.
A RAC control console with vacuum pump, dry gas meter, a calibrated orifice, and
inclined manometers completed the sampling train.

Flue gas temperature was measured by means of a Type K thermocouple which was
connected to a direct readout pyrometer..  The thermocouple sensor was positioned
adjacent to the sampling nozzle.

Gas velocity was measured using a calibrated "S" type pi tot tube provided with
extensions and fastened alongside the sampling probe.  Gas stream composition
(carbon dioxide, oxygen, and carbon monoxide content) v/as determined utilizing
Orsat apparatus to analyze stack gas samples.  Gas stream composition proved
to be ambient air since no combustion products were found in any of the stack
gas effluent samples.

The test train used for'particulate sampling at the baghouse exhaust stack
location was  identical to the train described above except for a rigid
borosilicate connection  in place of flexible tubing between the filter
                                 - 10 -

-------
between the filter holder and the first impinger.  See Figure 5 for
train schematic.

Part i cle _5 ize Distribution Sampling Apparatus

                                                                      R
A stainless steel nozzle was connected directly to an 8-stage Anderson
cascade impaction device which separated the particles according to
their effective aerodynamic particle diameters.  A glass fiber filter
was used to capture any particles that passed through the impactor
substrates to permit the measurement of total particulate.  The filter
holder was maintained at stack temperature and was connected by Tygon
vacuum tubing to the first of four Greenburg-Smith impingers which were
included in the train to condense the moisture  in the gas stream.  All
impingers were maintained in a crushed ice bath.  A RAC control console
with vacuum pump, dry gas meter, a. calibrated orifice, and  inclined
manometers completed the sampling trai'n.

-------
0.75 TO 1 in.
           TEMPERATURE SENSOR
2:0.75 in.       PITOTTUBE


       TEMPERATURE SENSOR
                                                                              THERMOMETER
                                      TEMPERATURE CONTROLLED
                                      HEATED AREA
                      PITOT MANOMETER

                          ORIFACE
        REVERSE-TYPE
        PITOTTUBE
                                                                          \
                                                                         VACUUM GAUGE
                                                                MAIN VALVE

                                                                \
                                                              AIRTIGHT PUMP
                                                                                           CHECK VALVE
                                                                                                 VACUUM
                                                                                                 LINE
                             THERMOMETERS
                                                  DRY GAS METER
                              FIGURE  k  PARTICULATE SAMPLING TRAIN
                                         EPA METHOD 5
                                         BAGHQUSE INLET DUCT

-------
             , TEMPERATURE
               SENSOR
0.75 TO 1 in.
0.75 in.

    PITOT TUBE '
                  PROBE
                   .TEMPERATURE SENSOR
                                                                       , THERMOMETER
                                                                         •CHECK VALVE

                                                                          VACUUM  LINE

                                                                            VACUUM GUAGE
/THERMOMETER

   /HEATED AREA
          FILTER HOLDER
                                                                                           THERMOMETERS
          PROBE-(pi{
    REVERSE-TYPE
     PITOT TUDE
                                                                                                    ORIFICE
                                                                                                    AND
                                                                                                    MANOMETER
                 PI TOT MANOMETER
                                                                  ICE BATH

                                                       DISTILLED WATER
                     FIGURE 5  PART1CULATE SAMPLING TRA1N-EPA METHOD 5
                                                 EPA METHOD 5
                                            BAGHOUSE EXHAUST STACK

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                                              TEST PROCEDURES '

 Preliminary  Tests

 Preliminary  test data was obtained at each sampling  location.  Stack geometry
 measurements were  recorded and  sampling point distances calculated.  A  pre-
 liminary  velocity  traverse was  performed at each test  location utilizing  a
.calibrated "S"  type  pi tot tube  and a Dwyer inclined manometer to determine
 velocity  profiles.   Stack gas temperatures were observed with a direct
 read-out  pyrometer equipped with a chromel-a 1umel thermocouple.  Gas
 stream  composition and moisture content values were estimated from
 information  supplied by  Oxychem.

 Preliminary  test data was used  for nozzle sizing and nomagraph set-up for
 isokinetic sampling .procedures.

 Calibration  of  the probe nozzles, pitot tubes, metering systems, probe  heaters,
 temperature  gauges and barometer were performed as specified  in Section 5 of
 EPA  Method 5 test  procedures  (see Appendix E for calibration  data).

 Ammonium  Sulfate Dryer Baghouse Inlet Duct

 A  series  of  three  tests  were  conducted at the inlet,  to  the Ammonium Sulfate
 Dryer Baghouse  simultaneous with pฃ)rticulate  test runs at the exhaust  stack.1
 The  sampling was performed at one point of average velocity for a  total test
 time of 120  minutes.  This point was chosen before each test  by running a
 rough velocity  traverse  across  the open area of the duct.  Test data was
 recorded  every  five  minutes during all test periods.

 Table 1 presents a summary of test data for each of  the three runs.  Test
 result  summarization appears  on Table 3-

-------
One particle size distribution test was performed following the completion
of test run 3.

One sampling point located at a site of average velo'city was selected from
velocity traverse data for particle size distribution testing.   The gas
stream was sampled isokinetically at that point for k minutes which permitted
collection of sufficient  sample for analysis without overloading the filter
substrates.  Sample volume, temperature, and pressure data was  recorded
before and after the test.  See Figure 6 for a distribution plot.

Ammonium Sulfate Dryer Baghouse Exhaust Stack

A series of three EPA Method 5 tests were performed at the Ammonium Sulfate
Dryer Baghouse exhaust stack simultaneous with the inlet test runs.  Eight
points were traversed, 4 per port axis, for 15 minutes each yielding a test
period 120 minutes in length.

During particulate sampling, gas stream velocities were measured by  inserting a
calibrated "S" type pitot tube into the stream adjacent to the sampling nozzle.
The velocity pressure differential was observed  immediately after positioning
the nozzle at each point, and  sampling rates were adjusted to maintain isokinetic
sampling.  Stack gas temperatures were also monitored at each point with  the
pyrometer and thermocouple.  Additional temperature, measurements were made at
the final  impinger and at the  inlet and outlet of the dry gas meter.

Test data was recorded every five minutes during all test periods.  Table 2
presents a summary of test data for each of the  three runs.  Test result
summarization appears on Table A.

Visible emissions observations were recorded concurrently with each particulate
test repetition by a certified observer according to EPA Method 9 procedures.
See Table  k for result 'summary.

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                                                   ANALYTICAL PROCEDURES


Particulate Sample Recovery


At the conclusion of each test, the sampling trains were dismantled,
openings sealed, and the components transported to the field laboratory.

Sample integrity was assured by maintaining chain of custody records
which will  be supplied upon request.


A consistent procedure was employed for sample recovery:


      o   The glass fiber filter(s) was removed from its holder with
          tweezers and placed  in its original container (petri dish),
          along with any loose particulate and filter fragments (Sample 1).

      o   The probe and nozzle were separated and the internal particulate
          rinsed with acetone or distilled water into a borosilicate container
          while brushing a minimum of three times until  no visi'ble particles
          remained.  Particulate adhering to the brush was rinsed with acetone
          or water into the same container.  The front half of the filter
          holder was rinsed with acetone or water while brushing a minimum
          of three times.  The rinses v/ere combined (Sample 2) and the
          container sealed with a Teflon lined closure.

      o   The total liquid in  impingers one, two and three was measured,
          the value recorded, and the liquid discarded.

      o   The silica gel was removed from the last impinger and immediately
          weighed.

      o   Acetone  and distilled water samples were retained for blank
          analys i s.


Particulate Analyses


The  filters (Sample 1) and any loose fragments were desiccated for 2k hours and
weighed to the nearest 0.1 milligram to a constant weight.
                                - 16 -

-------
The acetone and distilled water wash samples (Sample 2)  were evaporated
(acetone at ambient temperature and pressure;  water at 105 C and ambient
pressure) in tared beakers, and desiccated to constant weight.   All  sample
residue weights were adjusted by the acetone or water blank values.

The weight of the material collected on the glass fiber filter(s)  plus the
weight of the residue of the nozzle/probe/front-half filter holder washes
represents the "total" EPA Method 5 catch.  Complete laboratory results
are presented in Appendix B of this report.

Particle Size. Sample Recovery and Analyses

The cascade impactor substrates and any loose fragments were carefully
removed from their support plates with tweezers and placed in individual
containers (petri dishes) for shipment to Weston Laboratory.

Each cascade impactor filter was fired at 525 C and pre-weighed to the
nearest 0.1 milligram to constant weight at Weston1s Laboratory prior
to on-site application.   Subsequent to emissions exposure, the cascade
impactor substrates, back-up filters and any loose fragments (Sample ^i)
were desiccated for 2k hours in the Laboratory, and weighed to the nearest
0.1 milligram to constant weight.
                                - 17 -

-------
                                              DISCUSSION OF TEST RESULTS

Participate test data and test result summaries are presented in Tables 1
through A of this report.  Figure 6 illustrates the particle size
distribution of the participate matter at the baghouse inlet location.

No unusual process operating conditions were encountered during any of
the test periods.

A heavy build up of particulate matter covered approximately 68% of the
inside area of the baghouse inlet duct at the test port location and
therefore precluded particulate/velocity traversing of the duct cross-
sectional area as specified in EPA testing methodology (see Figure 2).
Sampling at a single point of average velocity proved to be the most
feasible testing alternative (the blockage could not be easily removed)
and was the procedure followed for all three inlet tests.   Therefore,.
since no part iculate/veloc-i ty traversing could be performed as required
to insure representative sampling, the inlet test results should only
be viewed as a rough guide when evaluating the performance efficiency
of the bag collector.

The amount of particulate matter discharged to the atmosphere from the
baghouse was <_ 0.093 grains/dscf and ฃ Q.Jk pounds/hour.  The certified
observer recorded no visible emissions emanating from the stack during
the test program.  However, water droplets containing dissolved particulate
matter were frequently observed dripping from the stack during the test
periods.  This phenomenon was due to water vapor condensation on the  inside
walls of the stack due to cooling the gas stream below the saturation
temperature.

The particulate removal "efficiency of the baghouse was mediocre averaging
roughly 95-3%.

                                 - 18 -

-------
                       D
Results of the Anderson  cascade impaction particle size distribution test
conducted at the baghouse inlet site showed a perponderance of relatively
large particles entering the collector (90% of the particles, by weight,
were _>_ 2.2 y in diameter).   Visual  inspection of a sample collected from
the baghouse indicated the presence of many large product granules.

It is suspected that the high grain loading measured at the outlet
location was due to a malfunction in the baghouse.  Consequently, the
plant was contacted, the baghouse corrections were made, and three
additional tests were run at the baghouse outlet location at a later
date.  The inlet duct was not tested during this period since most of
the internal area of the duct was filled with an irregular buildup of
product solids at the test site which prevented representative sampling.
Since the entire unit would have been required to shut down to enable
the inlet duct to be cleaned a decision was made to test the outlet
location only.
                                 - 19 -

-------
                                            OCCIDENTAL  CHEMICAL  COMPANY
                                                    Hous ton ,  Texas

                                                      TABLE  1

                                     AMMONIUM  SULFATc DRYER  BAGHCUSE  INLET  DUCT
                                                  Sunrcary of  Te^st^ Data_
Test Para

   Tes t Number
   Test Date
   Test Period

S a n p 1 i _n c _D j t a

   Samp ling Duration, mf nutts
   Nozzle Dia"-.-ter,  inches
   Baronetric Pressure, Inches mercury
   Average Orifice Pressure Differential,  inches water"
   Average Dry Gas Temperature at Meter, ฐF
   Samp Ie Vo!une at  Meter Conditions, cubic  feet
   Somp I e Vo I ume at  Standard Conditions,   cubic

Gas Strga.n Mo if. tu/e  Content

   Tola J Water Collected by Train, ml
   Standard Volume of Water Collected, cubic  feet
   Moisture  In Cos Stream, percent by volume
   Mole Fraction of  Dry Gas

Gas _S t r e; a m Compos it i o n

   C02, percont by vof'jme
   Oo, percent by vol urne
   CO, percen t by vo! u.~e
   N'2 , percent by vo I UiT.e
   Molecular Weight  of Wet Gas
   Molecular Weight  of Dry Gas

Gas Stream Veloci t_y_
   Static Pressure,  inches water
   Absolute Pressure,  Inches mercury
   Average Temperature,  F
   Pttot Tube Calibration Coefficient
   Total Number of Sa;np! ing Points
   Velocity at Actual  Conditions,  feet/second

GasS t ream Vo t erne t r ic^_F 1 oy/

   Stack Cross-Sect Ional Area,  square feet
   Volumet rIc FIow at  ActuaI Cord 11 ions,  cub ic  fee t/m i nute
   Vol umetf" ic Flow at  Standard  Conditions,  cubic  feet/minute

Percent  Isokinot ic






wa t e r

feet

















ie t/m i nutc
feet/™inute
1
9/12/73
O9'i0-1230
120.0
0.125
2S-77
0.55
86.
50.33
^9-37
156.
7.3^
12.9
0.871
0.0
20.9
0.0
79.1
27-55
28.97
- 2. it
29.59
153-
0.831
1.0
103.
0.21
1 ,300.
960.
2
9/12/73
1350-1620
120.0
0. 125
23.77
0.55
89.
W.37
<<7.27
I'd .5
6.66
12.lt
0.876
0.0
20.9
0.0
79.1
27:62
28.97
- 2.8
29-56
176.
0.331
1.0
105-
0.21
1 ,320.
950.
3
9/13/78
0315-1225
106.0
0. 125
29.79
0.55
89.
!<2.
-------
                                            OCCIDENTAL CHEMICAL COMPANY
                                                  Houston, Texas
                                                     TABLE 2
                                   AMMONIUM SULFATE  DRYER SAGHOUSE EXHAUST STACK

                                                 Sumnary  of Test Data
Test Data

   Test Number
   Test Date
   Test Period

Samp I in-; Data

   Sampling Duration, minutes
   Nozzle Diameter,  inches
   Barometric Pressure, inches mercury
   Average Orifice Pressure Differential, inches water
   Average Dry Gas Temperature at Meter, ฐF
   Sample Volume at Meter Conditions, cubic feet
   Sample Volume at  Standard Conditions,   cubic feet

Gas Stream Moisture  Content

   Total Water Collected by Train, ml
   Standard Volume of Water Collected, cubic feet
   Moisture in Gas Stream, percent by volume
   Mole Fraction of  Dry Gas

Gas Stream Composition

   CG"2, percent by volume
   0^, percent by volume
   CO, percent by volume
   (12, percent by volume
   Molecular Weight  of Wet Gas
   Molecular Weight  of Dry Gas

Gas Stream Veloci tv

   Static Pressure,  inches water
   Absolute Pressure,  inches mercury
   Average Temperature,  F
   Pitot Tube Calibration Coefficient
   Total Number of Sampling Points
   Velocity at Actual Conditions, feet/second

Gas Stream Volumetric Flow
                                                                   9/12/78
                                                                  0940-1230
                                                                  120.0
                                                                    0.189
                                                                   29-77
                                                                    0.69
                                                                   85.
                                                                   56.60
                                                                  186.
                                                                    S.76
                                                                   13.7
                                                                    0.363
                 2
              9/12/73
             1350-1620
             120.0
               0.185
              29.77
               0.60
              39.
              52..-8
              51.03
               6.83
              11.8
               0.882
               9/13/7S
              0915-1225
              120.0
                0.189
               29-79
                0.55
               87.
               5L27
              1<*7.5
                6.9
-------
                                       OCCIDENTAL  CHEMICAL  COMPANY
                                             Houston,  Texas
                                                TABLE  3  '
                                  AMMONIUM  SULFATE  SAGHOUSH INLET  DUCT
                                        Senna ry  or  Test  P.esu } t s
Test Data
Test Murnber
Test Dace
Test Time
Gas Flow
Standard Cubic Feet/minute, dry
Actual Cubic Feet/minute, wet
Par t i cu I a t S5
Nozzle, Probe and Front Hair" Filter Holder Catch Fraction, g
Filter Catch Fraction, g
Total Pa.-t iculates, g
Particuiote Emissions
Grains/dry standard cubic foot
Pounds/hour
Baghouse Participate Removal Efficiency, percent
Product Moisture Content
Moisture content of Dryer Inlet Sampla, percent
Moisture content of Dryer Outlet Sample, percent
1
9/12/78
OSAO-1230
960.
1 ,300.
2.7212
0.520^
3. 2*116
1 .01
8.36
97.2
0.46
0.14
2
9/12/78
1350-1620
950.
1,320.
2.5637
0,3817
Z.W*
0.96
7.31.
91.1
0.50
0.19
3
9/13/73
0915-1225
950.
1 ,320.
7.2971
2.3?21
1.0.2S92
3-33
31.2
97.6
0.54
0.03
 Based on Total  P^rticulates captured by t ra i n.

Standard Conditions - 68ฐ? and 29-32 inches mercury.

-------
                                     OCCIDENTAL CHEMICAL  COMPANY
                                           Hous con,  Texas
                                              TA3LE It
                            AMMONIUM S'JLFATE  DRYER BAGHOUSE EXHAUST STACK
                                       Sunimarv of  Test  Results
Test Data
Test Number
Test Date
Test Ti.ne
Gas Flow
Standard Cubic Feet/minute , dry
Part i cut act's
Mo:;lc:, Probe and Front Half Filter Holder Catch Fraction, g
Filter Catch Fraction, g
Total Part iculates , g
Particulate Emissions
Grains/dry standard cubic foot"
Pounds/hour
Saghouse Particular Removal Efficiency, percent
Visible Em i s s i on s
> S percent opacity, minutes observed
0 percent opacity, ninutes observed
No visible emission, minutes observed
Product Moisture Content
"loir.ture content of Dryer Inlet Sample, percent
Moisture content of Cryer Outlet Sample, percent

1
9/12/78
09^0-1230

930.
> o:! A
i , .iou .
0.059!)
0.0
-------
                           AMMONIUM SULFATE  DRYER BAGHOUSE  INLET
                                 Particle Size  Distribution
                                          FIGURE  6
10 0
q n
y . u
8 0
7 n
/ . u
A n
in b'U
ฃ en
o
.— i. n
r= H .U
F, ••? n
uu
2:
- u • /
o 0 A
CC
^ n q

uu ,
-=. n L.
K
CJ
uj n ^
u_ u • •>
u.
• LU
00
. i.
0.1
































































































































/
/
/
/










/
/
/
/
r









/
/
/
/
/














i







































































































-










































































































































O.fll   0.05 0. 1 0.7  0.5  I
 2C  30   40 50   60  70   80
CUMULATIVE  PERCENTAGE

 (%  Weight  
-------
 APPENDIX A




RAW TEST DATA

-------
PRELIMINARY VELOCITY TRAVERSE	—-  .- ...
PLANT. LAY ^•VJU-...-
DATE' ^ - ^ v--"^
LOCATION -XnWV- -4r-, P^Vซ-'O
STACK I.D.
BAROMETRIC PRESSURE. JR. Hg -."•'S
STACK GAUGE PRESSURE, in. H70 - "- • ~\
L 1
OPERATORS O'AxV...; 11 1 Me, In >\^,v

TRAVERSE;-
POINT
NUMBER ,

r\/ I 0
,A 1 • J
• . | ,3^
/ •LJ-
/ , -^5"










N

••'. '

r* - ' '**A< '.



• 'V •
.^ -.-*•""
'AVERAGE
VELOCITY
HEAD
Ups), in.H20

Z3.<#
'Lf\
2 . ฐ
3 f (^
TTT7'] 	
• "2,
-------
                     TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
F'LANT
DATE .
SAMPLING LOCATION _-
INSIDE OF FARULLTO
   OUTSIDE  OF PORT. (DISTANCE A) __Ul_
INSIDE OF NEAR WALL TO       x - t '
   OUTSIDE  OF PORT. (DISTANCE BiTl?	
STACK I.D.. (DISTANCE A - DISTANCE Bi -^ '
NEAREST UPSTREAM DISTURBANCE __<3^L"j+-_
NEAREST DOWNSTREAM DISTURBANCE	31
CALCULATOR   O'/OoJ / I	

                                                                  SCHEMATIC OF SAMPLING LOCATION
N o-r-c. '
TRAVERSE
POINT
NUMBER
Xv /
1 *
d
y
s
t
! 7
%
7
fo

/#
•












*z, A,'~, -> 7
FRACTION
OF STACK 1.0.















-'





..-

'
•
0- /ป 2u.
STACKi.O.
-,.
















..







•~^ ccxjevcA vnj/
PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1 8 INCH)
•
\
\ /
\/
A
/ \
/ \
/ \
/ \
/ \
/
,--"
* *




...
•"






r
\
DISTANCE B





' ,




\














"\ • JO.^-t rj '•-' "/ j'\
TRAVERSE p'oiNT LOCATION
FROM OUTSIDE OF PORT
(SUM OF COLUMNS 4 & 5)
* ... 	 	 	 -J








• '•:•' -'• - , '
:•• ' '

' V
'• /' .A:ป '
' v% • 1 "
--' ^.. ""*-"-.'*.',











-------
                      NOMOGRAPH DATA
PLANT




DATE _
SAMPLING LOCATION  ^ ^ I   7i-i



CONTROL BOX NO.
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEfviPERATURE i AMBIENT + 20 ฐF). ฐF
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. Hg
(Pmฑ0.073 x STACK GAUGE PRESSURE in in. H20i
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD. in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE ^p. in. H20
^H,5
Tmavg.
Bwo
pm
ps
Ps?
rm
savg.
^avg.
•^Pmax.
r/,t
o./
O.A
8.*
13^
Jb*
7-/o
-—, ...-4
*- / ซ ^
-T..A
/,o
/75
a. 5
Kb
)'6
3^
i /'


-------
                            PRELIMINARY VELOCITY TRAVERSE
PLANT__
DATE	1
LOCATION
BAROMETRIC PRESSURE, in. Hg	__'i_
STACK GAUGE PRESSURE, in. HoO  ..-T---\.-V
QPFRATORS   c '/:? .•-' -' •   /	''  ' •.' •/,'..
                                                         SCHEMATIC OF TRAVERSE POINT LAYOUT
TRAVERSE
POINT
NUMBER
>' ~ /
i
C-
'J>
V
















x



AVERAGE -
VELOCITY
HEAD
Dps), in.H20
X -A
. '79
. <^^
. ^!
i
) •-

-!-•"












';


-
, 7.<
STACK
TEMPERATURE
v '

















/'



TRAVERSE
POINT
NUMBER

v' — .''
^•^
•'1
_. /




















AVERAGE
VELOCITY
HEAD
!ApsK in.H20

. . ;< ^
O ")
- 7,;
, •//



/ — •

















STACK
TEMPERATURE
(Ts). ฐF

/ ? "•
-j
/..U
.' -•-. ~>






















-------
TRAVERSE  POINT LOCATION  FOR CIRCULAR  DUCTS
PLANT      ---^ •':j_C_>.:V-.vs--.
DATE .  ..   "'3 — ^ -'. ~".-\	
SAMPLING LOCATION	>'••.. c,.-c •
INSIDE OF FAR 'AALL TO
   OUTSIDE OF  PORT. (DISTANCE Ai._
INSIDE OF NEAR WALL TO
   OUTSIDE OF  PORT. (DISTANCE B! _
STACK I  0.. (DISTANCE A - DISTANCE 3..
NEAREST UPSTREAM DISTURBANCE	
NEAREST DOWNSTREAM-DISTURBANCE._
CALCULATOR	sJ.?jy_
-------
                      NOMOGRAPH DATA
PLANT
DATE.  "
SAMPLING LOCATION
CONTROL BOX NO.  _
                   4 V
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20ฐF).ฐF
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. HI
(Prnฑ0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD, in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL. NOZZLE DIAMETER, in.
REFERENCE .ip. in. H20,. ' .--
AH,:,
Tmavg.
BWO
Pm
-\'l ;V
ps
Pspm
savg.
^Pavg.
•^Pmax.
• .9
3/s*
V*
/. t
/• v'0
/ -"i ซC*
/ -""' ,'
— >
/o •*
-L^.l
30. \
/.o
/*>r
- 7y
. ^/
r*ซ
6>




-------
FIELD DATA
/- -• ', • '
1 '
1 '
1
j
)
" '.) ..
i i
.(
' f.
• i
ji
t;-
, fj:
T
W. .la
• t J. t-C-
^ if^oi-
r
ij
.1
*
\
\
\
\
f
>•'. •>
DATE i t'lc-1 *
SAMPLING L
SAMPLE TYP
RUN NUM3EF
t I OPERATOR _
3CATION 4-'iV. J. fj.
E Pcv-4 >o.l<-^ -
i O/vQ
O'-'Oe,'//
• ,i/* V"


>..;.•• .'•"•ป — ' ABSENT TEMPERATURE -VO ฐ r~ . H ซ | } '-'.

TRAVERSE
POINT .
NUMBER
X i
-



^ ' ' ' /
>y
\>-

<••!.-.;)
'*


li •?">








\ • 1 i. •;

BAROMETRIC
STATIC PRE
FILTER HUM
\. CLOCK TIKE
^v (24 hr
' \CLOCX)
TIME. .Tim X^
~C5 — — •---ฃฃ/ ^ฃj )
5
/D

D (-
>O
v>' m;iฃ'
vj ';
vi '
KJ
.. 1
•' '
PRESSURE 1- *' >1 1
SURE. (P ) *• ?-7JL._
",FR (5) --^ '^"/ . t '-\l..^L ''._"•-

GAS METER READING
S. (^ T) . / ^ -^
•S t ? . ^
<"/CN ,.^ 0
S"7-^-j O'^o
5" ' /5., / ^ o
5 -'/'/. '•>
o '7?: • 7'2o /--."/
•: /' '. '.'• <.'• :.--
.r ;; •<, ,,
jf y~ f
<7 -"/ / r \ Q \ ,
•
f5 0 >7 . ^ o (9
/,,/;5. 'AtD
(. •'(")'/ / f-> T'
(f (jtf . "'. '('• O
/...//. -:> .jo
(;'.> ( "''.. ,/,'. I •-'
^.jf'...-,!:'iป
if 1 7,r-'//<-|

to
READ AEiO REC
VELOCITY
HEAD
a . ^ j



- "r ' ";-"' -' .
''. n &ฃ


„• '/.-;''"''
(O.7,lfl
' .
ORO'ALL DATA EVERY
ORIFICE PRESSURE
DIFFERENTIAL
lilH). in. M20l
DESIREO
CT
C f
r c

: * ' •
"1 ''"I


. ฃ> '-'
; ••;
•;•'•.••/> //;/:• • "•• >
7S;'/l_>y










M. •-
'*
I "•' "'
i -"' ^
. ••: •'•,•

, y>
, 5'f
. ^-:;
,--;<
' ••- -/
- x
, •"' ^>
,;v >

ACTUAL
























-' • ฐ MIMUT

STACK
TEMPERATURE
(TS,."F
\1L{-
/ ^- y
/ <-/ ^
/ '•//
/'•'"
>.',?
'*. '
? Y
C; /
/ /
i / '•'
." ,' "-i
%' -'
~ ~FJT/ T-VAT
rr-; p.---
/ "7 :'•

OUTLET
*v
,\V)
3 3
i V
. f
i ) \ ;

;-" ...'
. ' - ,
.•'• i
V" i 	
f''".-
,-_"". 'f
^ -T
.''i" ' >
<"' ••'
'v '"•''
v" •/
*?< V/
/>' -':
'" ' "i
- --' "". - !
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f • , .
VP
, '• •

,

1
1
-. i

' ;":
'• .-'. •
:!*)••:

'<••!•' " ^ _J ' --' ' '• -
                                                  "V.c--
                                                           s

-------
                                                                                        FIELD DATA
PLANT i ••''"..":  •"-•/'--V--'A
DATE	'// 'If. 7.'L
SAMPLING LOCATION,   Q'->'1
                                                              J
                                'I''"^SAMPLE TYPE.
                                     RUN NUMBER _
                                     OPERATOR 	
                                     AMBIENT TEMPERATURE _"-1.
                                     BAROHETRIC PRESSURE   7-  :?
                                     STATIC PRESSURE. (Ps)..	^- .
                                     FILTER NUMBER is) ,.   "-'  -\.
PROBE LENGTH AND TYPE j	._•_:
NOZZLE I.D. _   _^:';6    :-.•<•-
ASSUMED MOISTURE.".._.  /O
SAMPLE BOX NUMBER	
METER BOX NUMBER _	{ ~ •?.;./ ..
MCHH AH.,.	/.-.:/-i;.'.
C FACT OH.!__..;. .;:
PI TOT  TUBE FACTOR	
REFERENCE Ap    .x
NOTE 	
                                                                         READ AND RECORD ALL DATA EVERY	._-.._  MINUTES
./ /  -J. r;;
TRAVERSE
POINT .
NUMBER
x •







!

•'•


	






	
\N CLOCK TIME
SAMPLING \^ CLOC'KI
TKi'E.min "S^
- — -^Xฃ/_ฃL






'••







//;} S'



GAS MET Eli READING
(Vml. I.3
;,6^ f'.;', {">
VELOCIIY
HEAD
(JipJ. in. H70
i t
- .- i
• ^
/•• •• • ! .'

- ,;•
- / •• ! '. •'-


-- ' ' ' '; !
• • -
IS
/ . . ' ' !
.-/' ' ' . ''
' ' ".' /
f
("* ^j . 1 - V */ '"


....... •._!_-, ,.
,•• /I"
Lฃ?Lฃ?





';, ,-,-' r-.'i •
! 	 ! "-..I I -;_! I..I • ! 	 : • .1 fj_
-. j / . 't " . r'. • M rr-; •• i
TV': r _• \ ("
"j l".J i'_, j I 	 f •
•'• '-.o ;i..n '-.o ':~...
I ;..'J '. ' "' :-j J ' .!..' :-.i..' :.J I :...i
Ul I"- '•ฃ> CO '••-' K.1 ••!-


1


.... ' >"l
-..
ORIFICE PRESSURE
DIFFERENTIAL
lilHI. in. H,0l
DESIRED 1 ACTUAL

f
.
, '• •


.16


-,














STACK
TEMPERATURE
|TS)."F






/ "V ' /'






1 -•._! \U
i -1 • CO OJ
r '.^ j --. ! flj ;""; : 	 r ': '• ;' . \
1 •!.'./ '" J' "' -i • :-:- C!j Oj ': ("j ' .'!.' '•! !
/ i":
DRY GAS METER
TEMPERATURE
INLET
77




	 -- -; -







..•j i-1- '--.I
j'' -I':-- PO
... :
OUTLET
11 -out1'"1
' .- '_ "



' . •








i"' •:. '
PUMP
VACUUM.
m. Hg




_ . ..: . ._
- 	



i
0 • " i
SAMPLE BOX
ItMPERAIURE.
"•'F











	
—
•
—
IMPINGER
TEMPERATURE.
"F


^ -


j











-••- 	



	

-------
TRAVERSE
POINT.
NUMBER
- / ;
/ •• /
•'







\



	

















i
\, CLOCK TIKE
S^'ป<\^ซ,
1 lint, mm x^
~~~^ — -J-L^


.^•'


• • •





























GAS METER READING
'V- "3
..'ป'•
' •' !
S-7'3^. 0"
• v . •. .
:~ ' ' \ v

.,;,- ' ; ;.-'
-, ''-•' '<• . •' :

/ ." '' ,
- -.
,'
1

' , -J ' ft

s ^,253 ^ 	



















VELOCITY
HKAO
iiipsl in H^O
'' /
-V-:
/ ''/,',
^'
-


/



"•' '
i
,7iT/



















1 ORIFICE PRESSURE
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                                 SUMMARY
                       RECORD OF VISIBLE EMISSIONS
Type oT Plant   y  'v
Company f'aire    O-: '-<
Plant Address    \-
                                                   Date
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                                                   Hours of Observation  ~C
                                                   Observer __ fi , L • _:vv^-c
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                                         '
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Background Description   *~^_ '• -\   \
Heather:  Clear   V0vercas,tr"   Partly Cloudy    Other       ',  S ky C o 1 o r & • /'^ <^l ;T',
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v:5
..;•;•
•" "i
,\j
*J
:'s"'
v
.Vj
\ ,
-v
\^,




COUNTS


• ./ ' "'""••' --. '- '•'•• v. 1~V- x--^r^



.

V\ '-\ .t?V. ^-'\ ' '-ฐv =ป ? -'/ ( •-•'..
^ j)

,'

V^^l'-.T^-f- J^,^ .^^ ?^.-V->ฃ-W f.s;,c ^rtr. •"-
( Cv+fcVrrJ,} Jr> ^-vฐ - ^-i
1 7/C C / ? 0 • ? 7- *?6-
1 ?7D,C)O^./\ V^Ir>
i „ 	 — — ^
l._^=, — . 	 _^_ 	 < 'v i
i


•
"l- w^-ffc-f





-------
    APPENDIX B  .




LABORATORY REPORTS

-------
                                      ANALYTICAL DATA
 PLANT_
 DATE „<
 SAMPLING LOCATION _4-H    :
             C   1 '     i
 SA.MPLE TYPE _l_5::lL'iLL,.lLli

 RUN fUJMBLR_._Q;:_L^=.
SAMPLE BOX NUMBER __1

CLEAN UP iMAN.._ !\-'-' '
                                                 COMMENTS:
F   'NT HALF

  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                                1  "^ U  "7
                                I  -^  •' v* I..

                                       .?
                                                 CONTAINER (J-L.
CONTAINER ^.-J....i
                           LABORATORY .RESULTS

                           "i """' D i   ^
                           \  , C\ -.   ;.'\    rrig
                                                                                           ng
                                                FRONT HALF SUBTOTAL
                                                                                           ffi
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS, AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS,
    AND BACK HALF OF FILTER HOLDER
ETHER-CHLOROFORM
EXTRACTION
CONTAINER "" '
BACK HALF SUBTOTAL
mg

mg

TOTAL WEIGHT '

Jj^> F ) >, b m&
'
MOISTURE

  IMPINGERS      ,, f *
   FINAL VOLUME _2ฃlฃl_ ml
   INITIAL VOLUME ^^	ml
   NET VOLUME   	L.^ *r.,_ ml
  SILICA GEL
   FINAL WEIGHT
   INITIAL WEIGHT
   NET WEIGHT
                    ,
                  \ ur
                   f4
                                     I
                                                            ItfZ-
            TOTAL MOISTURE
                              SUBTOTAL

-------
                                    ANALYTICAL DATA
 PL ANT _  	•;._

 DATE  _...   "...,__

 SAMPLING LOCATION

 SAMPLE TYPE 	
 RUN NUMBER	

 SAMPLE BOX NUMBER	

 CLEAN UP MAN
                        COMMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                       CONTAINER
                       CONTAINER l/'U " /
QZLAf
 ~f, -1F
                                               FRONT HALF SUBTOTAL
 LABORATORY RESULTS
   X' '.".  U.
	•..)   , i	.	rag
        7>
                                                    ,—v  r*.   /••)
                                                    M  ^."}
                                                                                       .""•I
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS. AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPiNGERS. CONNECTORS,
    AND BACK HALF OF FILTER HOLDER
                       CONTAINER	
                       ETHER-CHLOROFORM
                         EXTRACTION

                       CONTAINER	
                                              BACK HALF SUBTOTAL
                                               TOTAL WEIGHT
                               .me
MOISTURE

  IMPINGERS
   FINAL VOLUME
   INITIAL VOLUME
   NET VOLUME   .

  SILICA GEL
   FINAL WEIGHT
   INITIAL WEIGHT
   NET WEIGHT
ml
ml
ml
                               17.
                                  TOTAL MOISTURE
                             SUBTOTAL

-------
                                     ANALYTICAL DATA
PLANT.

DATE_
SAMPLING LOCATION __

SAMPLE TYPE 	/

RUN NUMBER	
SAMPLE BOX NUMBER __ I ____
CLEAN-UP MAN _____ .
                     <
                                                COMMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE, PROBE. CYCLONE (BYPASS),
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                                                CONTAINER C<>.
                                               CONTAINER
                                                                          LABORATORY RESULTS.
                                                FRONT HALF SUBTOTAL
                                                                                         .nig
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS, AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS,
    AND BACK HALF OF FILTER HOLDER
                                               CONTAINER	
                                               ETHER-CHLOROFORM
                                                 EXTRACTION

                                               CONTAINER	
                                                BACK HALF SUBTOTAL
 mg
.mg
"""
TOTAL WEIGHT
~> qucr LI
^ ,, ~ f 7^ • /
j.
nig

MOISTURE

  IMPINGERS
   FINAL VOLUME  ^!^1
   INITIAL VOLUME _
   NET VOLUME   _
                        ml
                        ITll
                                     ' S
                                  /rs"'r>
  SILICA GEL
   FINAL WEIGHT
   INITIAL WEIGHT _ฃi
   NET WEIGHT     /J-
                              SUBTOTAL
                                                            TOTAL MOISTURE

-------
                                    ANALYTICAL DATA
PLANT ___.__t^lJ:_:
                X
DATE	
                       e
                     :AJ>-->-
SAMPL1NG LOCATION

SAMPLE TYPE 	

RUN NUMBER	
SAMPLE BOX NUMBER

CLEAN-UP MAN	
                                               COMMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE, PROBE. CYCLONE (BYPASS),    CONTAINER
    FLASK. FRONT HALF OF FILTER HOLDER

  FILTER NUMBER   ~2l{?:?~'    	      CONTAINER
                                                                          LABORATORY RESULTS
                                               FRONT HALF SUBTOTAL
                                                                                '.. "V ป...W... mg
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS, AND BACK
    HALF OF FILTER HOLDER

ACETONE 'WASH OF WRINGERS. CONNECTORS,
    AND BACK HALF OF FILTER HOLDER
                                               CONTAINER	
                                               ETHER-CHLOROFORf/1
                                                 EXTRACTION

                                               CONTAINER	
                                               BACK HALF SUBTOTAL
                                                TOTAL WEIGHT
                                                                                         mg
MOISTURE

  IMPINGERS
   FINAL VOLUME  _.
   INITIAL VOLUME
   NET VOLUME

  SILICA GEL
   FINAL WEIGHT  _
   INITIAL WEIGHT J,
   NET WEIGHT   _
                     _
                   SM
                        ml
                        ml
                        ml
                  7*
                                                           TOTAL MOISTURE.
                                                                              7"
                                                                                  n
                                                                                 J
                              SUBTOTAL

-------
                                     ANALYTICAL  DATA
 PLANT _  - . :-L_lLQ.Lll_._'
 DATE _..   "..:-•„_.	:	;
 SAMPLING LOCATION ^_-_____
 SAMPLE TYPE	
 RUN NUMBER	
 SAV.PLE BOX NUMBER	
 CLEAN UP WAN	
                                              COfAMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE. PROBE, CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                                   ''   5?
                                   t> i 0
                                t~\
                                              CONTAINER'-
                                              CONTAINER
LABORATORY RESULTS

 '',  :"N	•' <  V  m g
                                                FRONT HALF SUBTOTAL   / Q ,  r^ ff ^ฃ
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS, AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS,
    AND BACK HALF OF FILTER HOLDER
                                              CONTAINER	
                                              ETHER-CHLOROFORM
                                                EXTRACTION

                                              CONTAINER	
                                                BACK HALF SUBTOTAL
                                                TOTAL WEIGHT
               mg
                                                                                       . mg
MOISTURE
WRINGERS       :;•; I n
 FINAL VOLUME _Zl__l_
 INITIAL VOLUME ""? \
 NET VOLUME     '  •' :"!
  SILICA GEL
   FINAL WEIGHT
   INITIAL WEIGHT
   NET WEIGHT
                        ml
                        ml
                        ml
                                                          TOTAL MOISTURE
                              SUBTOTAL

-------
                                     ANALYTICAL DATA
 PLANT_

 DATE __.   ' . . ..__' ..

 SAMPLING  LOCATION .

 SAMPLE TYPE	__

 RUN NUMBLfi	

 SAMPLE BOX NUMBER

 CLEAN UP MAN
                                                 CO!,"OTS:
  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).    CONTAINER.
     FLASK. FRONT HALF OF FILTER HOLDER
                 ---">  ••-ซ•  '""*• ^
  FILTER NUMBER  rf Ji'ฑl_l^_  	      CONTAINER
                                                                           LABORATORY RESULTS
                                                                              ^ '''', 7
                                                                             _o.i* I	m
                                                FRONT HALF SUBTOTAL    Slฐl  I  > I	mg
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS, AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS.
    AND BACK HALF OF FILTER HOLDER
CONTAINER	_.	
ETHER-CHLOROFORM
  EXTRACTION

CONTAINER	

BACK HALF SUBTOTAL
                                                                                         -fug

                                                                                         .mg
                                                TOTAL WEIGHT

                                                                                      \
                                                                                    •  t
                                                                                          m
MOISTURE

  WRINGERS
   FINAL VOLUME  .
   INITIAL VOLUME
   NET VOLUME   .

  SILICA GEL
   FINAL WEIGHT
   INITIAL WEIGHT	
   NET WEIGHT	
                        ml
                        ml
                        ml
                                                            TOTAL MOISTURE
                              SUBTOTAL

-------
I   I
                                                             Project No.
                                                            '  Book No
                                                       45
                                                   15"    9.5"?^?  _!-?-.tt'^'  ! 'i*51  ..^fL!^\.,ooj;3._G.<'b
• i i i r
: 	 -rrrn ~
' ~ ~ " " r i r i '
' i •' ! : .



__:..__. ..... . ..
i ! [ i ! L
i • i i n r
- ._rTT_.r r^
. i i '
r , i i : i

• < i'
i i i -
i n i
! | ! i
! ; •

_. ; — J...L... j — L._L — i-,-— ..'. — L--
• 1 UU_i r. LI f JJ
1 i 1 i I 1 M J
i ' T~ i 1 I ' i i
~! i i i i '• ' '•
i ' ! TO Pri P '.* Ti'o 	 _
  Witnessed & Understood by me.
                                   Dale
                                   *) - 1
Invented by
s	
                                               Recorded by
                                                                                 Date,

-------
                              ฃ/ OO /-/ f      <^fv
TITLE	
Project No.
  Book No.

-------

-------
TITLE
T&A-^j  3-iT-r/i  sr:
'reject No.
 Book No.

-------
     APPENDIX C




SAMPLE CALCULATIONS

-------
                                SAMPLE CALCULATIONS
Test Run   1  "  Ammonium Sulfatc Dryer Baghouse Exhaust Stack
1.   Volume of dry gas sampled at standard conditions (63ฐF, 29-92
    in. rig) ,  dscf .
     m
      (std)
                         17.647  x  Y  x  V    x     P,   +
                                           m       \  b
                                      ( T    +   460 }
                                      *•  m           i
                                                       i             0 69  >        54.94
                         17.647  x  1.006    x 56.60  x f 29-97   +
                                                       \
    V ,                                     '           \             -3.6  /
    vm(std)          =   	

                                        (85-4+  460


    Where:

    V /  ,v          =   Volume of gas sample measured by the dry gas meter,
                         corrected to standard conditions, dscf.

    V                =   Volume of gas sample measured by the dry gas meter at
                         meter conditions, dcf.

    P.                =   Barometric pressure, in.  Hg.

   ^>H               =   Average pressure drop across the orifice meter,
                         in.  H20.

    T                =   Average dry gas meter temperature, ฐF.

    17-647            -   Factor that includes ratio of standard temperature
                         (528ฐR) to standard pressure (29.92 in. Hg).ฐR/in. Hg.

    Y                =   Dry gas meter calibration factor.


2.   Volume  of water vapor in the gas sample corrected to standard conditions, scf.

    Vw(std)          =  (0.04707 x  V.J +  0.04715
    Vw/stdj          =  (0.04707  x 172 ) +  (0.04715 x   14    )       8.76

    Where:

    V /   ,\          =   Volume of water vapor in the gas sample corrected to
                         standard conditions, scf.

    V                =   Volume of liquid condensed in impingers, ml.
     we

-------
                                       - 2 -
    W
     wsg
    0.0^(707
Weight of water vapor collected in silica gel, g.

Factor which includes the density of water
(0.002201 '.'-/ml), the molecular weight of water
(18.0 1b/1b-mole),  the ideal gas constant
121.85  (In.  Hg} (ft3)/(lb-moie)(ฐR)j ; absolute
temperature at  standard conditions  (528ฐR), absolute
pressure at standard conditions (29-92  in. Hg),  ft  /ml
    0.0^715
Factor which includes the molecular weight of water
(18.0 Ib/lb-mole), the ideal gas constant
[21.85 (in.  Hg)(ft3)/(lb-mole)(ฐR)j .  absolute
temperature at standard conditions (528ฐR) , absolute
pressure at standard conditions (23-92 in. Hg), and
A53-6 g/lb, ft3/g.
3.   Moisture content.
     ws
                                 w
         (std)
                          w(std)        m(std)
    B
     ws


    Where:

    B
     ws
         8.76
    8.76 + 5k.3k
                             0.137
Proportion of water vapor, by volume,'  in the gas
stream, dimension less.
 .   Mole fraction of dry gas.
                         1 - B
                              ws
    M
1  -  0.137 =  0.863
    Where:

    M .
Mole fraction of dry gas, dimension 1 ess
5.  Dry molecular weight of gas stream,  Ib/lb-mole.
    MW
0.^0(?oC02)   +  0.320 (W2)  + 0.280
                                            +  % CO)

-------
                                       - 3 -





    MWd              =   (O.VtO x      )+ (0.320 x      ) +[0.280 (      +       )]





                          28.97  (Air)





    Where:



    MW,              =   Dry molecular weight, Ib/lb-mole.




    ^CO-             =   Percent carbon dixoide by volume, dry basis.





    %0~              =   Percent oxygen by volume, dry basis.





    'fcNj              =   Percent nitrogen by volume, dry basis.



    %CO              =   Percent carbon monoxide by volume, dry basis.



    O.kkO            =   Molecular weight of carbon dioxide, divided.by 100.



    0.3'20            =   Molecular weight of oxygen, divided by 100.



    0.280            =   Molecular weight of nitrogen or carbon monoxide,

                         divided by 100.





6.   Actual  molecular weight of gas stream (wet basis), Ib/lb-mole.



    MW               =    'MW,  x  M .')   +    [18   (1 - M )]
      s                      do'                  d




    MW               =    (28.97x0.863)    + D8  0 -0-863;]



                           27-46





    Where:



    MW               =   Molecular weight of wet gas, Ib/lb-moie.



    18               =   Molecular weight of water, Ib/lb-mole.





7-   Average velocity of gas stream at actual conditions, ft/sec.             ,


                                                            !      s  (avg)

                          85.^9 x C   x   ( / :.p)
    's                             P             av9-  x       p	Z—MTT—

-------
                                                               ^qi
                          85.^9   xO.8^3 x  0.769x            "
                                                       _  30.09

                     = '   ^6.9

    V/here :

   -,_,-                =   Average gas stream velocity,  ft/sec.


    85.A9            "   Pitot  tube  constant,  ft/sec   X

                         (ib/lb-moleHm.HgM
                         . 1"ฐP)  (in.'  H20)'  '_  '

    C                =   Pitot  tube  coefficient, dimens ion 1 ess .


   i, p               =   Velocity head of stack gas,  in  FLO.

    T                =   Absolute  gas stream  temperature,   R.

    P        '        =   Absolute gas stack pressure,  in.  Hg.


8.   Average gas stream dry volumetric flow rates, dscf/min.


    n                    1058.8  x  -v   x  A   x  M ,   x   P
    <*s(std)  •        =   -- S- -  s -- ^ - ง-
                                           s

                         1.058.8  x ^6.9 x  O.^^9x  0.863x  30.09   '
    Mstd)                         "TTJl  +  ^i60)

                     =   980.

    Where:

    Q /   ,N          =   Volumetric flow rate of dry  stack gas,  corrected  to
                         standard conditions, dscf/min.
                                                          2
    A                =   Cross-sectional area of stack,  ft .

    1058.8           =   Factor which  includes  standard  temperature  (528ฐR) ,
                         standard pressure  (29-92  in.  Hg) , and  60  sec/min,
                         (ฐR)  (sec)
                         (in. Hg) (min)
9-  Isokinetic variation calculated from  intermediate  values,  percent.

-------
                                       - 5 -

                         17-316  x  T    x  V
                                             m(stdj	
                                                        2
                         V   x  6  x  P   x  M ,  x  (D )
                          s            s      d       n
    I                 =   17.316 x  531  x   5^.94
                         ~wTs   x  fio  x 30.09"  O63x( o. 189 )2

                         107.8

    Where:

    I                 =   Percent of isokinetic sampling.

    Q          •       =   Total sampling time, minutes.

    D                 =   Diameter of nozzle, inches.

    17-316           =   Factor which includes standard temperature  (528ฐR) ,
                         standard pressure  (29-92 in. Hq),  the formula for
                         calculating area of circle 1"^ D              .     -
                                                    —r—   , conversion of

                         square feet to square inches (  1^'0, conversion of
                         seconds to minutes  (60),  and conversion to
                         percent (100),  (in. Hg)  (in2) (min) .

                                        (ฐR) (ft2)  (sec)

10.   Particulate concentration, gr/dscf.

    C]                =   0.015^32 x M
                                     m(std)

    C                =   0.015^32  x   	^^	    =  0-028
     1                                      5^.9^
    Where:

    C,                =••  Particulate. concentration, gr/dscf.

    M                =   Total weight of particulate caught by train, mg.

    0.015't32     .    =   Conversion factor of gr/mg.


11.   Particulate mass emission rate, Ib/hr.

    PMRt             =   0.00857^  x  C1  x  Qs(std)


                         0.0085714  x 0.028  x  980    =  0.24

-------
                                   - 6 -
Where:

PMR              =   Particulate mass  emission  rate,  Ib/hr.

0.008571A        =   Conversion  factor relating  minutes  to hours  (60),  and
                     grains  to pounds  (7,000).(lb)  (n>in)/(gr)  (hr) .

-------
        APPENDIX D




EQUIPMENT CALIBRATION DATA

-------
                                                                        ;c     r  "•• .^
                                                                          s/t--. i-
Da te
      Barometric  pressure,
                                                           Box Hn
                            .in. tig        Dry gas meter !lo. 1
Or i f ice
manonie tcr
setting ,
All,
in. 1(20
0.5
1.0
2.0
•Z^rtf
1-Sjxtf'
8.0
Gas volume
wet test
meter
vw.
5. cos
xSVaCG.
xrv*?.i
/ ซ "' ' V
^n" T J .^ i/ '. &?
10
Gas volume
dry gas
meter
S-041
J- 7ฃ
/O/.O
/33f0

Time
0,
mi n
njl.
'7.65C
13, /U
1.15s
7C-V5b

Average
Y
,?7Y<
AllQ
/ '^>?"t
/.?2SJ /,7/? 7
/.ocj A8?*ป
/.co 6
,r/-?^

/1006
/,905
/. 7 r-?

/,77fe
Ca1cula t ions



All
0.5
1.0
2.0
f^rCT

8.0


AM
1176
0.0360
0.0737
0.147
0.294
0.431
0.503
Y
Vw Pb (td + 460)

V^(pb + iirs) (tw+ 46ฐ)






,IILB
0.0317 All f(tw ^ 460) el 2

Pb (td -i- 460) 1 V 1
u w L_ W J






    Y = Ratio of accuracy of wet test meter to dry test meter.  Tolerance = ฑ 0.01
      = Orifice pressure differential  that gives 0.75 cfm of air at 70ฐ F and 29.92

        inches of mercury, in. I^O.   Tolerance - - 0.15

-------
                                                                     ,s
                                                                        --   .002.
     Date
Box Mo.
Barometric pressure, Pb = 	 in. llg • Drv gas meter ilo. ff/Vj?/
U
Or i f ice
manometer
setting ,
AH,
in. H20
0.5
1.0
2.0
'5.0
,S>rCr
8.0
Gas volume
wet test
meter
V
S.ooo
Xitftft
1 0 * @Qj
] Q , C 0 0
-Mf.oot
10
Gas volume
dry gas
meter
// (9 f? 
I0,5k(
s.^.^

Tempera ture
Wet test
Meter
ฐF
7^^l_j
7// 7-tLj
7-f _22
73 _
73 73

Dry gas
Inlet
ฐF
'7Z.
xlฃl
^3
jH^
/D 2-

Outlet
ฐF
70
^Z
rTfr
Vfjf
*%&.


fiie ter
Average
ฐF
H.o
?y,7ฃ>
gฃj>
96.2^
Time
0,
min
/?.6^
#2^
i?,W'j?
?.?&
^5" IT! 5^3
Average


Y
/.^r
8.0


AH
1576
0.0360
0.0737
0.147
0.29-1
0.431
0.503
Y
Vw Pb (td + 460)
vd(pb + rf-e) (*ซ + 46ฐ)






AH@
0.0317 AH f(tw + 460) el 2
7bTtd~~46o) [~"v; -J






    y =  Ratio of accuracy of wet test meter  to dry test meter.  Tolerance  =  i 0.01
   h'g  =  Orifice pressure differential  that gives 0.75 cfm of air at 70ฐ  F  and 29.92
        inches of mercury, in. I^O.   Tolerance •- i 0.15

-------
     Date
                                                    Box No.
Barometric pressure,
                                  in.  Hg
Dry gas meter Do.	
Ori f ice
manometer
setting ,
ill.
in. M20
0.5
1.0
2.0
4.0
6.0
8.0
Gas volume
wet test
meter
V
5
5.0^0
10
10
10
Gos volume
dry gas
meter
f ^3
•7 ซ./ / ,* i t "C
t • it
/ / . , .•

	 i
Temperature
Wet test
Meter
ฐF

7 ฐ "> 6
70 7ฐ
~> (i
. u


Dry gas
Inlet
d i *
ฐF

^\\_
';iv
"->,


Outlet
ฐF

5C^/^_
^ "*^r- /
'~'~S.' ,.


meter
Average
ฐF
eo-c
5S.S
^rj.
^7!


Time
o,
mi n
0^
1C3^
Y
3
1,01
I3,6~?iuo6
9 /==/:


Average
(.Do




\ ^ *\
fe 'U 'sJs
3 ^ ,03
4- <3u 1 ฃ


1^ t
Calcula tions



AH
0.5
1.0
2.0
4.0
6.0
8.0


AH
ITTe
0.0360
0.0737
0.147
0.294
0.431
0.588
Y
Vw Pjj (tj •ป• 460)

^ + rare) (^ + 46ฐ)






AH,
0.0317 AH f(tw + 460) el 2

Pb (td + 460) [ vw J






      = Ratio  of  accuracy  of wet  test meter to dry test meter.  Tolerance = ฑ 0.01
      =  Orifice  pressure differential that gives 0.75 cfm of air at 70ฐ F and 29.92
        inches of mercury,  in. f^O.  Tolerance - ฑ 0.15

-------
       O
Date_

                         3,0, Q
Barometric pressure,  PL  =	in.  llg
                                                          Box No.


                                                Dry  gas meter Mo.
Calculations

Orifice
manometer
setting ,
All.
in. H20
0.5
4-^,5
-5-rsaS
4.0
6.0
8.0


Gas volume
we t tes t
meter
v.'m
5
' lf''%^
44- S
AM';10
10
10


Gas volume
dry gas
meter
V
7/t,.O^5"
to i . nz$
> i /i
o%' ; . AS 7





Wet test
Meter
ฐF
/cHvo






Tenipe
i)
Inlet
d i *
ฐF
^?
7V
?~~^.




-a ture
ry gas
Outlet
ฐF
?r~
^ i
*^~rj





me ter
Average
"F
A-'./r
* i f
' ' *, ; ^.-:



Average


Time
0,
min
13 ^^r
3 C^(J !>,>
i/3 .ฃ3
A7S7-






Y
l,^
t.oi^
Uf*



|.6\


All
' i -S3
_J Ji^
5 i^Jt



W 1.8^,



AH
0.5
1.0
2.0
4.0
6.0
8.0


AH
1376
0.0360 '
0.0737
0.147
0.294
0.431
0.508
Y
Vw Pb (^ + ^0)

Vd(Pb + f576j (tw + 460J ;.




-

A 11(3
0.0317 All -f(tw 4 460) e] 2

Pb (td + ^60} [ Vw




1
i

   ,Y =  Ratio of accuracy of wet  test meter to dry test meter.  Tolerance = ฑ 0.01
      =  Orifice pressure differential that gives 0.75 cfm of air at 70ฐ F and 29.92
        inches of mercury,  in. f^O.  Tolerance - - 0.1T>

-------
Date..

Barometric pressure,
                                   in.  llg
          Box Ho.

Dry gas meter ilo.

Or i f ice
manometer
setting ,
Ail.
in. !I20
0.5
1.0
2.0
4.0
6.0

3.0

Gas volume
wet test
meter
vw.
ft3
5
5,
10
10
10

Gas volume
dry gas
meter
vd •
ft3
IlfJ&a
pii5"^
'-Trr.'/"^?



10 |
Temperature
Wet test
Meter
wป
ฐF
7V
7V

?v >v




D
Inlet
(J 1 *
ฐF
3^
*'^V.
i! C




ry gas
On 1 1 e t
t-do '
ฐF
^ J
T6 ^
^6/C




me ter
—
Average
t(J •
ฐF
sy

T ime
0,
m i n
&3S
j? ? I0?//]
.^C7




i&i's







Y



AHp
/.^ 1*11
/.ocg 7,83
^•.T




• ~ • • '1
Average / t*-*)^ /'
"ฃ ( .^fT




X™ N ซ^-
\ . o ^>
Calculat ions


AH
0.5
1.0
• 2.0
4.0
fi.O
8.0

;
All
1376
0.0360
0.0737
0.147
0.294
0.431
0.508
Y
Vw Pb (*d 4 <160)
Vd.(Pb - nIJ-6) (tw + 460)



•>


aii(3
0.0317 All [{t,.. -f 460) el 2
PbTt d~~4 6 6 ) [ V~ _






    Y = Ratio oY accuracy of wet test meter to dry test meter-.  Tolerance = ฑ 0.01
      = Orifice  pressure., differential that gives 0.75 cfm of air at 70ฐ F and 29.92
        inches of  mercury,  in.  J.^O.   To'lerance - ฑ 0.15

-------
           Date.
Barometric pressure,
                                       in. Hg
          Box No.

Dry gas meter No.
0.7

Or i f ice
manometer
setting ,
ill,
in. II20
HJ^S-
•4UL
2.0
4.0
6.0
8.0

Gas volume
wet test
meter
V
5
5
10
10
10
10

Gas volume
dry gas
meter
•~s •,- "/ r* " ••.
'./ -; '





Wet test
Meter
ฐF
/ * /-
^V ->v




Tempe
D
Inlet
ฐF
GC'J





•a Lure
ry gas
Ou t 1 e t
ฐF
c l5N'j>
AC





meter
Avo'"a ge
tt|,
ฐF
"•5 < !
//





T ime
0,
m i n
•'0.1'
/0,?o



..

V
A CปC
/roc?



	


ซ• '.77
c, i . Tl


"
.

                                                           Average
     Calcula t ions




AH
0.5
1.0
2.0
4.0
6.0
8.0

A It
AH

13.6
0.0360
0.0737
0.147
0.294
0.131
0.508
Y
Vw Pb (fcd 4 ^0)

ii /n i -i' 1 /t L /^nl
V4Pb + 13767 (tw + 460J






	
Al!|3
0.0317 AH Rt,. -f 460) 8] 2
1
/ 4 -\ \ 1
Pb (tcj 4 -IbO) L VW J






           = Ratio of accuracy of wet test  meter to  dry  test  meter.   Tolerance = * 0.0)
           = Orifice pressure differential  that  gives  0.75  cfm of  air at 70ฐ F and 29.92
             inches of mercury,  in.  HjO.   Tolerance  -  -  0.15

-------
R Y \-> V_. v
CH.KD BY
PROJECT
SUBJECT
J 0 A TF ^
DATF

P ; Vo i:
I 2- ( / / .JrJT


T^ W <
H"^ ^^_j/ .*ป^ซ.t ^,~%V* >
v_-s. \\ Vo r -5.-
rlSHFFT OF
WO NO

V\o- "f-^c.'to^S
                        0.
                                           V
                                                    .S^o  .21,1
T
VJ

-------
         APPENDIX E




DETAILED BAGHOUSE INFORMATION

-------
xc.v.er.tai Chemical Company
                                                            September 27,  1978
           Mr. Berry Jackson
           Ray F. Western, Inc.
           West on Way
           Westchester, Penn. 19330

           Dear Sir:

           There were 17 tons per hour produced on the  12  and  13th.

           Enclosed are the production and spec sheets  your  requested.

           Please return the spec sheets.

           Thank you.

           Sincerely yours ,

           OCCIDENTAL CHEMICAL COMPANY
              cu-i
           R.E. Kleissle
           Production Manager
              9802  Lawndale   P. 0. Box 5337    Houston, Texas 77012    (713) 477-8811

-------
                                  HOUSTON SULFATc
                      Tons
                                     Srorf -
                          O
                                     Finish -
               Tofal -
                            SPARGER PRESS:  High  ,^_T
                                                            Low
                                                                  Flushing Every
                                                        10   12   14   16   18   20  23   F
;ed ch AM AM PM PM
3
/6
A'
/->
,~
— .
                      Ton 5
                                     Start -
                                            SPARGER PRESS: 'High  :•:
                                     Finish - /^ 7'
                                                            LOW
               Toi-a! ~ /•
PJB:._.._Avorpge;   ^7. -Q   J.P.H.
                                                                  Flushing Every
                             8   10   12   14   16   18   20  28   F
ked af: AM AM PM PM
/
'3
'3
'1
/j>
_--
>*?
a^?
/ ^;
      I d ?  ^
Tons
                                     Srarf -
                                     Finish -
Total -
      Average:  / 7, q    T.P.H.
                                            SPARGER PRESS: High
                                                            Losv
             8     10   12   14   16
                                                          20  28   F
CHeckocI ah AM AM PM PM
u
li
fa
.-^
^
—
/^_
/'-L
//
                /"

                      Tons
                               THIS MONTH:
                                                  Tons
          AVERAGE
           T.P.H,
                    Y.T.D.
Tons

-------
                                                                    DATE:
                                      HOUSTON  SULFATE
\m
; V

 Start -
                                SPARGER PRESS: High
                                         Finish-
                          Tons
                                                Lov/
MffRKS:    Average:   //? 2_  T.P.H.
                                                     --1 r-r
                                                    ฃ^_/._
                                                                     Flushing Every   ^
                  8   10   12   14    16   18   20  28   F
^•checked ct: AM AM PM PM
ซ!•• ,.. ..,,_T1.__T^ 	 , 	 r— 	 •- 	 . 	 	 	 .
/
If
//
/ป-
/s-
-—
/?/-
if 2
u?i:- .

X ^
/ ^/O, & Tons

Start - (0
Finish - /--C/O /$//
Total - /--/. 0 ,vj^/
ฃฃ"•
SPARGER PRESS:
Flushing Every
High s-?
Low ^
6—
/
^

                              T P'H
                  8    10   12   14   16    18   20  28   F
Oil- checked at:      AM
                            AM
PM
      PM
                                                                         //

        /: x-:
HI FT 3   '*j^J>?'..?J...<^ f-^.
E.fijปRKS:  Average:  ///7    T.P.H.
    Start -
                                         _F_m?sh.- JH, / tf .?,

                                         Total - /i/ / ^ -7.
          ?*'
                              SPARGER PRESS: High
                                                 Low
                                                                      Flushing Every
                  8    10   12   14   16   18   20   28   F
|งl Checked at: AM AM PM PM
2
;z.
o
/7
/T
• _
i*
13

A^TY  TOTAL:   V,^. t/   Tons


JtH 2URt-.Y AVERAGE
                  THIS MONTH:
                                       / /  7 —
                                                                                          Tons
                                	T.P.H.
                        Y.T.D.
                                                   Tons

-------
     APPENDIX F




PROJECT PARTICIPANTS

-------
                                              PROJECT PARTICIPANTS
The follov/ing Weston employees participated in this project:
Peter J.  Marks
Laboratory Manager
econENVIRONomics Division
Barry L.  Jackson
Supervisor,. Air Testing

Jeffrey D. O'Nei11
Project Scientist Assistant
econENVIRONomics Division
econENVIROMomics Division
Gregory Celi ano
Assistant Project Scientist
econENVIRONomi cs D i v i s i on
Richard J, Urban
Laboratory Technician
econENVIRONomics .Division
David D. Maloney
Laboratory Technician
econENVIRONomics Division

-------
     \,v
                               cer
                                                   tifies  tnat
                                            &\RRY  L,  JACKSON
                                           ia6  completed
                               VISIBLE EMISSIONS EVALUATION SEMINAR
               Date:
T. ftl
                         .' 71
                                                             Dale:
DIRECTOR, CENTER FOR AIR
  ENVIRONMENT STUDIES
                                                                          Recertified:
                                                                                                   Date:
                                                                      VICE PRESIDENT FOR
                                                                    CONTINUING EDUCATION

-------