&EPA
            United States
            Environmental Protection
            Agency
            Office of Air Quality
            Planning and Standards
            Research Triangle Park NC 27711
EMB Report 78-NMM-8
March 1979
            Air
Clay

Emission Test Report
Georgia Kaolin
Dry  Branch, Georgia

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    SOURCE EMISSIONS TEST REPORT

        GEORGIA KAOLIN COMPANY
         Dry Branch Georgia

      #8 Raymond Impact Mill
               and
            Roller Mills
                         ROY F. WESTON,  INC.


                         Lb.O'/LM
                         V. D. O'Neill
                         Assistant Project  Scientist
                         Barry Lr
                         Supervisor Air Testing
     RFW  REPORT NO. 0300-81-06
     CONTRACT NO. 62-02-2816

     WORK ASSIGNMENT NO. 5
         Prepared by:

      ROY F. WESTON,  INC.
ENVIRONMENTAL CONSULTANTS-DESIGNERS
           Weston Way
  West Chester, Pennsylvania 19380
          (215) 692-3030

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                                                           TABLE OF CONTENTS
                                                                        PAGE
List of Tables and Figures                                              i, ii
Summary                                                                    1
Introduction                                                               3

Description of Test Locations                                              5
   No. 8 Raymond Impact Mill Baghouse Exhaust Stack                        5
   No. 8 Raymond Impact Mill Baghouse Inlet Duct         .                  5
   Roller Mills Baghouse Exhaust Stack                                     5
   Roller Mills Baghouse Inlet Duct                                        5
Description of Sampling Trains                                            11
   Particulate Sampling Trains                                            11
   Particle .Sizing Train                                                  13

Test Procedures                                                           15
   Preliminary Tests                                                      15
   No. 8 Raymond Impact Mill Baghouse Exhaust Stack                       15
   No. 8 Raymond Impact Mill Baghouse Inlet Duct                          16
   Roller Mills Baghouse Exhaust Stack                                    16
   Roller Mills Baghouse Inlet Duct                                       17
Analytical  Procedures                                                     18
   Particulate Sample  Recovery                                            18
   Particulate Analyses                                                   18
   Particle Size Sample Recovery and Analyses                             jg
 Discussion of Test Results                                               20
       t
 Appendix A - Raw Test Data
 Appendix B - Laboratory Reports
 Appendix C - Sample Calculations
 Appendix D - Equipment Calibration Data
 Appendix E - Project Participants       *
 Appendix F - Operations  Log

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                                              LIST OF TABLES AND FIGURES

TABLE
 NO.                      TfTLE                                     PAGE

  1             #8 Raymond Impact Mill Baghouse Inlet                 21
                Summary of Test Data

  2             #8 Raymond Impact Mill Baghouse Exhaust               22
                Summary of Test Data

  3             Roller Mills Baghouse Inlet                           23
                Summary of Test Data

  4             Roller Mills Baghouse Exhaust                         2k
                Summary of Test Data

  5             #8 Raymond Impact Mill Baghouse Inlet                 25
                Summary of Test Results

  6             #8 Raymond Impact Mill Baghouse Exhaust               26
                Summary of Test Results

  7             Roller Mills Baghouse Inlet                           27
                Summary of Test Results

  8             Roller Mills Baghouse Exhaust                         28
                Summary of Test Results

  9             #8 Raymond Impact Mill Baghouse Exhaust               29
                Particle Size Distribution

 10             Roller Mi 11 Baghouse Exhaust                          31
                Particle Size Distribution

 11             Roller Mill Baghouse Exhaust                          33
                Visible Emission Test 1

 12             Roller Mill Baghouse Exhaust                          34
                Visible Emission Test 2

 13             Roller Mill Baghouse Exhaust                          35
                Visible Emission Test 3

 1A             #8 Raymond Impact Mill Baghouse Exhaust               36
                Visible Emission Test 1

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FIGURE
 NO.                      TITLE                                     PAGE

  1              #8 Raymond Impact Mill Baghouse Exhaust                6
                Port and Sampling Potnt Locations

  2              #8 Raymond Impact Mill Baghouse Inlet     1            7
                Port and Sampling Point Locations


  3              Roller Mills Baghouse Exhaust                          8
                Port and Sampling Pomt Locations

  k              Roller Mill Baghouse Inlet                            10
                Port and Sampling Point Locations

  5              Particulate Sampling Train                            12
                EPA Method 5 - Mfsco.

  6              Particulate Sampling Train                            14
                EPA Method 5

  7              #8 Raymond Impact Mill Baghouse Inlet                 30
                Particle Size Distribution

  8              Roller Mills Baghouse Inlet                           32
                Particle Size Distribution
                                  i i

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                                                        SUMMARY

The Emission Measurement Branch of the U. S. Environmental Protection
Agency contracted Roy F. Weston, Inc. to conduct a source testing
and analysis program at the Georgia Kaolin Company's Dry Branch,
Georgia clay processing facility.

The primary objective of the testing program was to measure the
particulate emissions to the atmosphere from two baghouse-control led
sources at the plant (No.  8 Raymond Impact MM 1  and Roller Mills).
This objective was completed by performing a series of three particulate
tests utilizing EPA Method 5    procedures at each baghouse exhaust stack
                             s
location.  In addition, visual  determinations of plume opacities were
made simultaneously with each particulate test at both source discharge
                                (2)
points according to EPA Method 9    protocol.  Also, similar EPA Method 5
particulate and Anderson cascade impactor tests  were executed at both
baghouse inlet sites to measure the emissions and the particle size
distribution of the particulate matter entering  the bag collectors.

The particulate matter emission results are summarized below:.

            No. 8 Raymond Impact Mill Baghouse Exhaust Stack
Test                      Particulate Concentration     Particulate Emission Rate
 No.         Date         _ Grains/DSCF _     _ Pounds/Hour _
  1        12/6/78                 0.020                          2.49
  2 <      12/6/78                 0.012                          1.5^
  3        12/6/78                 0^016                          2.01
Series Average                      — •                           2.01
            No. 8 Raymond Impact Mill Baghouse Inlet Duct
Test                      Particulate Concentration     Particulate Emission Rate
 No.          Date        _ Grains/DSCF _     _ Pounds/Hour _
  1         12/6/78                k.53                         5*ป5.
                                 - 1 -
(!)Code of Federal Regulations, Title kO, Part 60, Appendix A, "Standards of
   Performance for New Stationary Sources," August 18, 1977-
   Federal Register, Vol. 39, No. 219, November 12,
' 'Run performed simultaneously with Test Number 2 at exhaust stack.

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                   Roller Mills Baghouse Exhaust Stack

Test                      Particulate Concentration     Partfculate Emission Rate
 No.         Date         	Grains/DSCF	'        	Pounds/Hour	

  1         12/5/78                 0.010                          0.73
  2        12/5/78                 0.005                          0.38
  3        12/6/78                 0.007                          0.48
Series Average                      —                            0.53

                   Roller Mills Baghouse tnlet Duct

Test         Date         Partfculate Concentration     Partfculate Emission Rate
 No.         Date         	Grafns/DSCF	     	Pounds/Hour	

  1         12/6/78                 1.76                        105.


The particulate removal efficiency of No.  8 Raymond Impact Mill  Baghouse was
measured at 99-72%, that of the Roller Mills was 99-54%.  Both efficiencies

were calculated based on one simultaneous tnlet/outlet test only.


No visible emissions were observed from either stack durfng the test program
with the exception of test run one at the Roller Mills exhaust stack where a

maximum of 5% opacity was observed.


Figures 7 and 8 illustrate the particle size distribution of the particulate

matter at the baghouse inlet locations.


Detailed summaries of test data and test results are presented in Tables 1

through 8 of this report.
                                 - 2 -


(U
   Run performed simultaneously with Test Number 3 at exhaust stack.

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                                                         INTRODUCTION

The Emission Measurement Branch of the U. S. Environmental Protection
Agency contracted Roy F. Weston, Inc. to conduct a source testing and
analysis program at the Georgia Kaolin Company's Dry Branch, Georgia
clay processing facility.  The objective of the testing program was to
measure various emission parameters from two milling operations at the
plant.

The locations tested, plus the number and types of tests performed at
each site, are listed below:

1.  No. 8 Raymond Impact Mill Baghouse Exhaust Stack
    a.  Three particulate tests by EPA Method 5.
    b.  One opacity test by EPA Method 9 simultaneous with Run One
        particulate test.

2.  No. 8 Raymond Impact Mill Baghouse Inlet Duct
    a.  One particulate test by EPA Method 5 simultaneous with one
        of the exhaust stack tests.
    b.  One particle size distribution test by cascade  impaction
                  D
        (Anderson  ).

3.  Roller Mills Baghouse Exhaust Stack
    a.  Three particulate tests by EPA Method 5.
    b>  Three opacity tests by EPA Method 9 simultaneous with
        each particulate test.

k.  Roller Mills Baghouse Inlet Duct
    a.  One particulate test by EPA Method 5 simultaneous with
        one of the exhaust stack tests.
    b.  One particle size distribution test by cascade  impaction
                  ^
        (Anderson  ).
                                 - 3 -

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All tests were conducted during the period 5"6 December 1978 by Weston
personnel and were observed by Mr. Dennis P.  Holzschuh, EPA Technical
Manager.

Test data and test result summaries are presented in Tables 1 through 8
of this report.   Particle size distribution results are shown in Figures 7
and 8.  Also incorporated herein ts a description of the test locations,
test equipment,  test procedures, sample recovery, and analytical methods
used during the test program.   Raw test data, laboratory reports, sample
calculations, equipment calTbratTon data, a list of project participants
and process operation logs are provided in Appendtces A through F,
respectively.
                                 - k -

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                                              DESCRIPTION OF TEST LOCATIONS

No. 8 Raymond Impact Mill Baghouse Exhaust Stack

Two V I.D. test ports, 90  apart, were installed on a straight section of
the 26" I.D. metal stack at a location 5-8 stack diameters (150M) downstream
and 1.5 diameters (AO") upstream from the nearest flow disturbances.  EPA
Method 1  criteria for this test locatfon requfred a minimum of 28 traverse
points.  A total of 32 traverse points (16 per axts) were sampled since
this number conveniently related to the desired test period length,   See
Figure 1  for port and samplfng point locations.

No. 8 Raymond Impact Mill Baghouse Inlet Duct

Two V I.D. test ports were placed at right angles on a straight section
of the 32"  I.D.  ductwork leading to the inlet of the baghouse at a
position greater than eight stack dfameters downstream, and greater
than two diameters upstream from the nearest gas stream flow disturbances.
Since the eight and two diameter crfterion were met a minimum of twelve
traverse points were required by EPA Method 1 regulations.  Figure 2
illustrates port and sampling point locations.

Roller Mills Baghouse Exhaust Stack

Two V I.D. test ports at 90  were placed on the 2V I.D. metal stack
5-5 diameters downstream and 2.2 diameters upstream from the nearest
flow disturbances.  Twenty sampling points (10 per axis) were selected
for testing.  See Figure 3 for port and sampling point locations.

Roller Mills Baghouse Inlet Duct

Two V I.D. test ports, 90  apart, were installed in a straight section
of the metal duct at a location which was 3.0 duct diameters downstream

                                 - 5 -

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                         GEORGIA KAOLIN COMPANY
                           Dry Branch,Georgia
                               FIGURE  1
                  #8 RAYMOND IMPACT MILL BAGHOUSE EXHAUST
                    PORT AND SAMPLING POINT LOCATIONS
                                                        40"
Port X
DUCT CROSS-SECTIONAL VIEW
Port Y
                                                        150"
Traverse
Point
Number
1
2
3
If
5
6
7
8
9
10
11
12
13
14
15
16
Distance from
Inside Near
Wai 1 , Inches
3/8
1-1/4
2-1 A
3-1A
4-3/8
5-3A
7-3/8
9-3/4
16-1/4
18-5/8
20-1/4
21-5/8
22-3/4
23-3/4
24-3/4
25-5/8
                                                                         O
                                  - 6 -

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                     GEORGIA KAOLIN COMPANY
                       Dry  Branch,Georgia
                           FIGURE  2
              #8  Raymond  Impact  M.i 11  Bag house Inlet
               Port  arid  Samplirig  Point  Locations
                   22'
                                 n  x
         Gas Flow

        , From

         Cyclone
O
To

Baghouse
32" I.D.
                 32" I.D
                                                       Traverse
                                                       Point
                                                       Number
                                                         1
                                                         2
                                                         3
                                                         iป
                                                         5
                                                         6
                Port Y

DUCT CROSS - SECTIONAL VIEW
                                  Distance  From
                                  Inside  Near
                                  Wai 1,  Inches
                                   1-3/8
                                   4-5/8
                                   9-1/2
                                 22-1/2
                                 27-3/8
                                 30-5/8
                               - 7 -

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                           GEORGIA KAOLIN COMPANY
                             Dry Branch,Georgia
                                 FIGURE 3
                         ROLLER MILLS BAGHOUSE EXHAUST
                      PORT AND SAMPLING POINT LOCATIONS
Port X
DUCT CROSS-SECTIONAL VIEW
Traverse
Point
Number
1
2
. 3
k
S
• 6
7
8
9
10
Distance From
Inside Near
Wai 1 , Inches
5/8
2
3-1/2
5-1/2
8-1 A
15-3 A
18-1/2
20-1/2
22
23-3/8
                                                        52"
Port Y
                                                                 n
                                                        132"
                                  o
                                                                                      roof
                                                                          From
                                                                         Baghouse
                                    - 8 -

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and 1.0 diameters upstream from the nearest flow disturbances.   A total  of
28 points were selected for test purposes,  1A per port axis.   Figure k
illustrates port and traverse point distances.
                                 - 9 -

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                        GEORGIA KAOLIN COMPANY
                          Dry Branch,Georgia
                              FIGURE  *ป
                      ROLLER MILLS BAGHOUSE INLET
                   PORT AND SAMPLING POINT LOCATIONS
   I  D
   FAN
To Baghouse
                      17-3/8" _LJL
  Port X
Port Y
Traverse
Point
Number
1
2
3
It
S
6
7
8
9.
10
11
12
13
14
Distance From
Inside Near
Wai 1 , Inches
1/2
1
1-3/4
2-1/2
3-1/2
4-5/8
6-3/8
11
12-3/4
13-7/8
14-7/8
15-5/8
16-3/8
16-7/8
             DUCT CROSS SECTIONAL VIEW
                                  -  10  -

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                                              DESCRIPTION OF SAMPLING TRAINS

Participate Sampling Trains
The test train utilized for participate sampling at both fnlet duct locations
and at #8 Raymond Impact Mill Baghouse exhaust stack location was the standard
EPA Method 5 train (see Figure 5).

A stainless steel nozzle was attached to a heated (^  250 F) borosilicate glass
probe which was connected directly to a borosilTcate filter holder containing a
V Reeve Angel 900 AG glass fiber filter.  The filter holder was maintained at
approximately 250 F in a heated chamber, and was connected by Tygon   vacuum
tubing to the first of four Greenburg-Smith impingers which were included in
the train to condense the moisture in the gas stream.   Each of the first two
impingers contained 100 ml of distilled water, the third was dry and the final
impinger contained 200 grams of dry pre-weighed silica gel.  The first, third,
and fourth impingers were modified Greenburg-Smith type; the second was a
standard Greenburg-Smith impinger.  All impingers were maintained in a crushed
ice bath.  A RAC control console with vacuum pump, dry gas meter, a calibrated
orifice, and inclined manometers completed the sampling train.

Flue gas temperature was measured by means of a Type K thermocouple which was
connected to a direct readout pyrometer.  The thermocouple sensor was positioned
adjacent to the sampling nozzle.

Gas velocity was measured using a calibrated "S" type pitot tube provided with
    A
extensions and fastened alongside the sampling probe.   Gas stream composition
(carbon dioxide, oxygen, and carbon monoxide content)  was determined utilizing
Orsat apparatus to analyze stack gas samples.   Gas stream composition proved
to be ambient air since no combustion products were found in any of the stack
gas effluent samples.
                                - 11

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    0.75 TO 1 in.
     I          TtlVU

   -A	^X
       TEMPERATURE SENSOR
                     K.


                      .	PROBE
    \
> 0.75 in.
           f
                                 TEMPERATURE CONTROLLED
                                 HEATED AREA
THERMOMETER
     PITOT TUBE


TEMPERATURE SENSOR
                              /
     PROBE    \
       V    V
                                  • STACK WALL
            REVERSE-TYPE
            PITOT TUBE
                         PITOT MANOMETER

                             ORIFACE
                                                                                             CHECK VALVE
                                 THERMOMETERS
                                               \
                                             DRY GAS METER
                                                                 AIR TIGHT PUMP
                                                                                                   VACUUM
                                                                                                   LINE
                                  FIGURE  5  PARTICIPATE SAMPLING TRAIN
                                            EPA METHODS - Ml SCO

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The test train used for participate sampling at the Roller Mills Exhaust
Stack was identical to the train described above except a rigid glass
connector was used between the back half of the filter holder and the
first impinger.  (See Figure 6.)

Particle Size Distribution Sampling Apparatus
                                                                      n
A stainless steel nozzle was connected directly to an 8-stage Anderson  cascade
impaction device which separated the particles according to their effective
aerodynamic particle dfamters.  A glass fiber filter was used to capture any
particles that passed through the tmpactor substrates to permit the measurement
of total particulate.  The filter holder was maintained at stack temperature
                           ^
and was connected by Tygon   vacuum tubing to the first of four Greenburg-Smfth
impingers which were included in the train to condense the moisture in the gas
stream.  All impingers were maintained in a crushed Tee bath.  A RAC control
console with vacuum pump, dry gas meter, a calibrated oriffce, and inclined
manometers completed the sampling train.
                                - 13 -

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        TEMPERATURE
           SENSOR
                                                                  THERMOMETER
                                                                    CHECK VALVE

                                                                     VACUUM  LINE

                                                                       ,VACUUM GUAGE
                                                                                     THERMOMETERS
REVERSE TYPE
 PITOT TUBE
            PITOT MANOMETER
                                 IMPINGERS
                                                             ICE BATH
                                                                                              ORIFICE
                                                                                              AND
                                                                                              MANOMETER
                                                  DISTILLED WATER
                 FIGURE 6 PARTICULATE SAMPLING TRAIN-ERA METHOD 5

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                                                        TEST PROCEDURES

PrelIminary Tests
Preliminary test data was obtained at each sampling location.  Stack geometry
measurements were recorded and sampling point distances calculated.  A pre-
liminary velocity traverse was performed at each test location utilizing a
calibrated "S" type pitot tube and a Dwyer Inclined manometer to determine
velocity profiles.  Stack gas temperatures were observed with a direct
read-out pyrometer equipped with a chrome1-alumel thermocouple.  Moisture
content values were estimated from information supplied by Georgia Kaolin.

Preliminary test data was used for nozzle sizing and nomagraph set-up for
isokinetic sampling procedures.

Calibration of the probe nozzles, pitot tubes, metering systems, probe heaters,
temperature gauges and barometer were performed as specified In Section 5 of
EPA Method 5 test procedures (see Appendix D for calibration data).

No. 8 Raymond Impact Mill Baghouse Exhaust Stack
A series of three tests were conducted at No. 8 Raymond Impact Mill Baghouse
Exhaust Stack to measure the concentration and mass rate of particulate
matter emissions.  Thirty-two traverse points, 16 per port axis, were sampled
for three minutes each resulting in a total test time of ninety-six minutes.

During particulate sampling, gas stream velocities were measured by inserting a
calibrated "S" type pitot tube into the stream adjacent to the sampling nozzle.
The velocity pressure differential was observed immediately after positioning
the nozzle at each point, and sampling rates were adjusted to maintain isokinetic
sampling.  Stack gas temperatures were also monitored at each point with the
pyrometer and thermocouple.  Additional temperature measurements were made at
the final impinger, inlet and outlet of the dry gas meter and at the
filter holder chamber.
                                - 15 -

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Test data was recorded every three minutes at each point during all test periods.
Leak checks were performed according to EPA Method 5 instructions prior to and
after each run and/or component change.  Table 2 presents a summary of test
data for each of the three runs.   Visible emissions observations were recorded
with Test Run 1  only due to lack of daylight during the other test periods.
Observations were performed by a certified observer according to EPA Method 9
procedures.  See Table 6 for result summary.

No. 8 Raymond Impact Mill Baghouse Inlet Duct
One EPA Method 5 test was performed at the inlet simultaneous with particulate
Test Run 2 at the outlet.  Twelve points were traversed, 6 per port axis, for
5 minutes, each yielding a test period 60 minutes in length.

Procedures for isokinetic sampling were identical for those described for the
outlet location except the test data was recorded every 5 minutes. Test data
and test result summaries are provided in Tables 1 and 5, respectively.

One sampling point located at a site of average velocity was  selected from
particulate traverse data for particle size distribution testing.  The gas
stream was sampled isokinetically at that point for 5 minutes which permitted
collection of sufficient sample for analysis without overloading the filter
substrates.  Sample volume, temperature, and pressure data was recorded
before and after the test.  See Figure 7 for a distribution plot.

Roller Mills Baghouse Exhaust Stack
    t
Three 120 minute Method 5 test runs were performed at the baghouse outlet.  A
total of 20 points were sampled for 6 minutes each per test.   Readings were
taken at 3 minute intervals.

Procedures for isokinetic sampling were identical to those described for
No. 8 Raymond Impact Mill Baghouse Exhaust Stack.
                                - 16 -

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See Tables k and 8 for test data and test result summaries respectively.

Visual determinations of plume opacity were performed by a certified observer
according to Method 9 Procedures.  A summary of results is presented in
Table 8.

Roller Mills Baghouse Inlet Duct
One Method 5 test was performed at the inlet simultaneous with particulate Test
Run 3 at the outlet.   Twenty-eight points were traversed, 1*t per port axis, for
2 minutes each yielding a test period of 56 minutes.

Isokinetfc sampling procedures were identical to those previously described
except that test data was recorded every 2 minutes.   Table 3 shows test data
summarization and Table 7 presents test results.

One particle size distribtuion sample was collected isokinetically at a point
of average velocity over a 3 minute period.  Sample volume, temperature, and
pressure data was recorded before and after the test.  See Figure 8 for
distribution results.
                                - 17 -

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                                                        ANALYTICAL PROCEDURES


Particulate Sample Recovery

At the conclusion of each test, the sampling trains were dismantled, openings

sealed, and the components transported to the field laboratory.  Sample in-

tegrity was assured by maintaining chain of custody records which will be

supplied upon request.


A consistent procedure was employed for sample recovery:


     •   The glass fiber filter(s) was removed from its holder with
         tweezers and placed in its original container  (petri dish),
         along with any loose particulate and filter fragments (Sample l).

     •   The probe (EPA 5) and nozzle were separated and the internal
         particulate rinsed with acetone into a borosilicate container
         while brushing a minimum of three times until no visible
         particles remained.  Particulate adhering to the brush was
         rinsed with acetone into the same container.  The front half
         of the filter holder was rinsed with acetone while brushing
         a minimum of three times.  The rinses were combined (Sample 2)
         and the container sealed with a Teflon lined closure.

     •   The total liquid in impingers one, two and three was measured,
         the value recorded, and the liquid discarded.

     •   The silica gel was removed from the last impinger and immediately
         weighed.

     •   An acetone sample was retained for blank analysis.


Particulate Analyses

The filters (Sample 1) and any loose fragments were desiccated for 2k hours and

weighed to the nearest 0.1 milligram to a constant weight.


The acetone wash samples  (Sample 2) were evaporated at ambient temperature and

pressure in tared beakers, and desiccated to constant weight.  All sample residue

weights were adjusted by the acetone blank value.
                                - 18 -

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The weight of the material  collected on the glass fiber filter(s) plus the
weight of the resfdue of the acetone nozzle/probe/front-half filter holder
washes represents the "total" EPA Method 5 catch.  Complete laboratory results
are presented in Appendtx B of this report.

Particle Size Sample Recovery and Analyses
The cascade impactor substrates and any loose fragments were carefully removed
from their support plates with tweezers and placed in individual  containers
(petri dishes) for shipment to the Weston Laboratory.

Each cascade impactor filter was fired at 525 C and pre-weighed to the nearest
0.1 milligram to constant weight at Weston's Laboratory prior to on-site
application.  Subsequent to emissions exposure, the cascade impactor substrates,
back-up filters and any loose fragments were desiccated for 2k hours in the
Laboratory and weighed to the nearest 0.1 milligram to constant weight.
                                - 19 -

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                                                   DISCUSSION OF TEST RESULTS

Particulate test data and test result summaries are presented in Tables 1
through 10 of this report.  Figures 7 and 8 illustrate the particle size
distribution of the particulate matter at the baghouse inlet locations.

No unusual sampling difficulties were encountered during the test periods,
but it should be noted that the two tests performed at the #8 Raymond
Impact Mill Baghouse on December 5, 1978 had to be repeated due to a
malfunction in the mechanical  collector which resulted in an abnormally
high particulate loading on the baghouse which invalidated the two tests.

The particulate removal efficiency of No. 8 Raymond Impact Mill  Baghouse
was measured at 99-72%; that of the Roller Mills was 99.5^%.  Both
efficiencies were calculated on one simultaneous inlet/outlet test
only.

                       ft
Results of the Anderson  cascade impactor particle size distribution
tests at both inlet locations show that _>_ 35% of the particles entering
each baghouse were >^ 1.0 microns in diameter.

Determination of visual opacity at the #8 Raymond Impact Mill Baghouse
resulted in no visible emissions observed with the exception of the first
test; similar observations of 0% opacity were made at the Roller Mill
Baghouse.  The first test at this location resulted in readings averaging
5% opacity.

The results of visible emission testing at both sites are summarized in
Tables 11 through 1A.
                                - 20 -

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                                                GEORGIA KAOLIN COMPANY
                                                  Dry Branch, Georgia

                                                       TABLE  1

                                        #8 Raymond  Impact Mill Baghouse  Inlet

                                                 Summary of Test  Data

Teat Data

   Test Number                                                               '
   Test Date                                                              12-6-78
   Test Period                                                           1615-1723

SampI Ing Data

   Sampling Duration, minutes                                             60.0
   Nozzle Diameter, inches                                                 0.188
   Barometric Pressure, inches mercury                                    29.98
   Average Orifice Pressure Differential,  inches water                     0.85
   Average Dry Gas Temperature at Meter,  F                               81.
   Sample Volume at Meter Conditions, cubic feet                          29-55
   Sample Volume at Standard Conditions, '  cubic feet                     28.64

Gas Stream Moisture Content

   Total Water Collected by Train, ml                                     'tS.S
   Standard Volume of Water Collected, cubic feet                          2.28'
   Moisture in Gas Stream, percent by volume                               7-''
   Mole Fraction of Dry Gas                                                0.926

Gas Stream Composition

   C02, percent by volume                                                  0.0
   02,  percent by volume                                                  20.9
   CO,  percent by volume                                                   0.0
   N2,  percent by volume                                                  79.1
   Molecular Weight of Wet Gas                                            28.16
   Molecular Weight of Dry Gas                                            28.97

Gas Stream Velocity

   Static Pressure, inches water                                         - 2.2
   Absolute Pressure,  inches mercury                                      29-82
   Average Temperature, ฐF                                               '36.
   Pilot Tube Calibration Coefficient                                      0.839
   Total Number of Sampling Points                                        12.0
   Velocity at Actual Conditions, feet/second                             51-3

Gas Stream Volumetric Flow

   Stack Cross-Sectional Area, square feet
   Volumetric Flow at Actual Conditions, cubic feet/minute
   Volumetric Flow at Standard Conditions,  cubic feet/minute

Percent Isokinetle                                                        98.5


Process Operations Data                                    See Appendix F for Operations Log
Standard Conditions  =  68ฐF, 29-92 inches mercury, dry basis.

                                                          - 21  -

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                                               GEORGIA KAOLIN COMPANY
                                                 Dry Branch, Georgia

                                                      TABLE 2
                                       #8  Raymond  Impact MM I Baghouse  Exhaust

                                                 Summary  of Test Data

Test Data

   Test Number                                                        1                  2                  3
   Test Date                                                       12-6-78            12-6-78            12-6-78
   Test Period                                                    OSS-IS'tO          1655-181*0          19*5-2130

Samp I ing Data

   Sampling Duration, minutes                                      96.0               96.0               96.0
   Nozzle Diameter, inches                                         0.180              0.180              0.180
   Barometric Pressure, inches mercury                             29-98             29-98              29-98
   Average Orifice Pressure Differential, inches  water              1-72              1.72               1.77
   Average Dry Gas Temperature at Meter,  ฐF                        95.                86.                76.
   Sample Volume at Meter Conditions, cubic feet                    69.07             69-89              73-32
   Sample Volume at Standard Conditions,  '  cubic  feet              65.0*             66.92              71.52

Gas Stream Moisture Content

   Total Water Collected by Train, ml                             10*1.5              120.0               87.5
   Standard Volume of Water Collected, cubic feet                  *-92              5-65               *ป.12
   Moisture in Gas Stream, percent by volume                       7.0                7-8                5.*
   Mole Fraction of Dry Gas                                        0.929              0.922              0.9*6

Cas Stream Composition

   C02, percent by volume                  .                        0-0                0.0                0.0
   03, percent by volume                                           20.9               20.9               20.9
   CO, percent by volume       .                                    ฐ-ฐ                ฐ-ฐ                ฐ-ฐ
   Nj, percent by volume                                           79-1               79-1               79-1
   Molecular Weight of Wet Gas                                     28-20             28-'2              28-37
   Molecular Weight of Dry Gas                                     28-97             28.97              28.97

Gas Stream Velocity

   Static Pressure, inches water                                   1.6                1.7                1.6
   Absolute Pressure, inches mercury                               30.09             30.11              30.09
   Average Temperature, ฐF                                        131.               1*1.               '*'•
   Pitot Tube Calibration Coefficient                              0.850              0.850              0.850
   Total Number of Sampling Points                                 32.0               32.0               32.0
   Velocity at Actual Conditions, feet/second                      80.0               81.2               81.7

Gas Stream Volumetric Flow

   Stack Cross-Sectional Area, square feet                         3-69              3-69               3.69
   Volumetric Flow at Actual Conditions,  cubic feet/minute      17,690.            17,960.            18,060.
   Volumetric Flow at Standard Conditions,  cubic  feet/minute   1*,790.            1*,650.            15,080.

Percent Isokinetlc                                                 95.6               99-3              103-1


Process Operations Data                                             SEE APPENDIX F FOR OPERATING LOG
Standard Conditions = 68 F, 29-92 inches mercury, dry basis.

                                                      - 22  -

-------
                                       GEORGIA KAOLIN COMPANY

                                         Dry Branch, Georgia

                                               TABLE 3
                                     Roller Hills Baghouse  Inlet

                                        Summary of Test Data

Test Data

   Test Number                                                         '
   Test Date                                                        ,\2'6
   Test Period                                                      1053-

Samp I ing Data

   Sampling Duration, minutes                                         56-0
   Nozzle Diameter, inches                                             0.188
   Barometric Pressure, inches mercury                                 29-98
   Average Orifice Pressure Differential,  inches  water                 2.4
   Average Dry Gas Temperature at Meter,  ฐF                           99.
   Sample Volume at Meter Conditions, cubic feet                       46.56
   Sample Volume at Standard Conditions,  '  cubic  feet                 43-28

Gas Stream Moisture Content

   Total Water Collected by Train, ml                                 79.0
   Standard Volume of Water Collected,  cubic feet                      3.72
   Moisture in Gas Stream, percent by volume                           ''ฐ
   Mole Fraction of Dry Gas                                            ฐ-921

Gas Stream Composition

   C02, percent by volume                                              ฐ-ฐ
   02,  percent by volume                                              20.9.
   CO,  percent by volume                                               ".0
   Nj,  percent by volume                                              79.1
   Molecular Weight of Wet Gas                                        28.10
   Molecular Weight of Dry Gas                                        28.97

Gas Stream Velocity

   Static Pressure, inches water                                      - 3-'
   Absolute Pressure, inches mercury                                  29-75
   Average Temperature,  F                                            '34.
   Pitot Tube Calibration Coefficient                                  0.839
   Total Number of Sampling Points                                    28.0
   Velocity at Actual Conditions, feet/second                          86.6

Gas Stream Volumetric Flow

   Stack Cross-Sectional Area, square  feet                             1-65
   Volumetric Flow at Actual Conditions,  cubic  feet/minute          3,550.
   Volumetric Flow at Standard Conditions,  cubic  feet/minute        6,960.

Percent Isokinetic                                                    94.9


Process Operations Data                                   See  Appendix F  for  Operations Log
  Standard Conditions  - 68ฐF.  29.92  inches  mercury,  dry  basis.

                                               - 23 -

-------
                                        GEORGIA KAOLIN  COMPANY

                                          Dry  Branch, Georgia
                                                TABLE 4
                                     Roller Mills  Baghouse Exhaust

                                        Summary of Test Data

Test Data

   Test Number                                                     1               2                3
   Test Date                                                     12-5-78        12-5-78          12-5-78
   Test Period                                                  0953-1203     1357-1605        1030-1252

SampI Ing Data

   Sampling Duration, minutes                                   '20.0         120.0            120.0
   Nozzle Diameter,  inches                                        0.189         0.189            0.189
   Barometric Pressure, inches mercury                           30.22         30.22            29-98
   Average Orifice Pressure Differential,  inches water             1.01          1.02             1.05  .
   Average Dry Gas Temperature at Meter, ฐF                      57.            73.              78.
   Sample Volume at Meter Conditions, cubic feet                 63-78         65.29            65.42
   Sample Volume at Standard Conditions, ' cubic feet             65-29         6^.79            63.87

Gas Stream Moisture Content

   Total Water Collected by Train, ml                           126.5         143-4             98.
   Standard Volume of Water Collected, cubic feet                 jj.96          6.75             ฃ.61
   Moisture in Gas Stream, percent by volume                      "•*           9-4              6.7
   Mole Fraction of Dry Gas                                      ฐ-9'6          0-906            0.933

Gas Stream Composition

   C02, percent by volume                                        ฐ-ฐ            0.0              0.0
   02,  percent by volume                                        20-9           20-9             20'9
   CO,  percent by volume                                         ฐ-ฐ            ฐ-ฐ              ฐ-ฐ
   N2,  percent by volume                                        79-'            79.1             79-1
   Molecular Weight of Wet Gas                                  28.05          27-93            28.23
   Molecular Weight of Dry Gas                                  28.97          28.97            28.97

Gas Stream Velocity

   Static Pressure, inches water                                 0-50           0.60             0.55
   Absolute Pressure,  inches mercury                            30.26          30.26            30.02
   Average Temperature, ฐF                                     129-           123-             136.
   Pitot Tube Calibration Coefficient                            ฐ-835          0.835            0.835
   Total Number of Sampling Points                              20.0           20.0             20.0
   Velocity at Actual Conditions, feet/second                    51-9           52.1             54.8

Gas Stream Volumetric Flow

   Stack Cross-Sectional Area, square feet                       3-14           3-14             3-14
   Volumetric Flow at Actual Conditions, cubic feet/minute   9,780.         9,830.          10,340.
   Volumetric Flow at Standard Conditions, cubic feet/minute 8,120.         8,150.           8,560.

Percent Isokinetic                                             108.0          106.8            100.2


Process Operations Data                             See Appendix F for Operations  Log
  Standard Conditions =68ฐ F,  29-92 inches mercury,  dry basis.

                                               - 24 -

-------
                              GEORGIA KAOLIN COMPANY
                                Dry Branch, Georgia
                                      TABLE 5
                      #8 Raymond Impact Mill Baghouse Inlet
                              Summary of Test Results
Test Data
   Test Number                                         1
   Test Date                                       12-6-78
   Test Time                                      J615-1723
Gas Flow
   Standard Cubic Feet/minute, dry               14,040.
   Actual Cubic Feet/minute, wet                 17,180.

Particulates
   Nozzle, Probe and Front Half Filter Holder         2.0415
           Catch Fraction,g
   Filter Catch Fraction, g                           6.3624
           Total Particulates, g                      8.4039
Particulate Emissions
                                 f\
   Grains/dry standard cubic foot                     4.53
   Pounds/hour                                      545.
 Based on Total Particulates captured by train.
O                        f\
 Standa'rd Conditions = 68 F and 29-92 inches mercury.

 Test conducted concurrently with Run 2, No. 8 Raymond Impact Mill Baghouse
 Exhaust Test.
                                   - 25 -

-------
                             GEORGIA KAOLIN COMPANY
                               Dry Branch, Georgia
                                     TABLE 6
                      #8 Raymond Impact Mill Baghouse Exhaust
                             Summary of Test Results
Test Data
   Test Number                                    1
   Test Date                                    12-6-78
   Test Time:                                  1355-1540

Gas Flow
    Standard Cubic Feet/minute, dry         14,790.
    Actual Cubic Feet/minute, wet           17,690.

Particulates
    Nozzle and Front Half Filter Holder
               Catch Fraction, g
    Fflter Catch Fraction, g
          Total Particulates,g

Particulate Emissions
    Grains/dry standard cubic foot
    Pounds/hour
    Baghouse Particulate Removal
         Eff i c i ency,pe rcen t

Visible Emissions
    5 percent opacity, minutes observed          0.0
    0 percent opacity, minutes observed         90.0
    Unobserved readings, minuted observed        0.0
0.020
2/49
           12-6-78
         1655-1840
        14,650.
        17,960.
              3
            12-6-78
          1945-2130
         15,080.
         18,060.
0.0381
0.0447-
0.0828
0.0228
0.0309
0.0537
0.0258
0.0460
0.0718
 0.012
 1.54

99.72
0.016
2.01
1
 Based on Total Particulates captured by train.
 Standard Conditions = 68 F and 29-92 inches mercury
3
 Opacity results listed are in minutes of the observed reading during the test period,
                                   - 26 -

-------
                          GEORGIA KAOLIN COMPANY
                            Dry Branch, Georgia
                                 TABLE 7
                       Roller Mills Baghouse Inlet
                         Summary of Test Results
Test Data
   Test Number                                            1
   Test Date                                            12-6-78
   Test Time                                          1053-12^0

Gas Flow
   Standard Cubic Feet/minute, dry                       6,960.
   Actual Cubic Feet/minute, wet                         8,550.

Particulates
   Nozzle, Probe and Front Half Filter Holder                l.*ป983
           Catch Fraction, g.
   Filter Catch Fraction , g                                 3.4416
           Total Particulates, g                             4.9399
Particulate Emissions
                                 2
   Grains/dry standard cubic foot                            1.76
   Pounds/hour                                             105.
 Based on Total Particulates captured by train.
 Standard Conditions = 68 F and 29.92 inches mercury.
 Test conducted concurrently with Run 3, Roller Mills Baghouse Exhaust Test.
                                   -  27  -

-------
                            GEORGIA KAOLIN COMPANY
                              Dry Branch, Georgia

                                    TABLE 8
                         Roller Mills Baghouse Exhaust

                           Summary of Test Results
Test Data

   Test Number
   Test Date
   Test Time

Gas Flow

Standard Cubic Feet/Minute,dry
Actual Cubic Feet/minute, wet

Particulates

Nozzle and Front Half Filter Holder
           Catch Fraction, g
Filter Catch Fraction, g
           Total Particulates, 9

Particulate Emissions
Grains/dry standard cubic foot
Pounds/hour
Baghouse Particulate Removal Efficiency,
           percent

Visible Emissions
    1
  12-5-78
0953-1203
8,120.
9,780.
>_ 10 percent opacity, minutes observed
 -  5 percent opacity, minutes observed
   0 percent opacity, minutes observed
     Unobservable reading, minutes observed
    0.010

    0.73
    .0.0
  112.75
    3-
    A.25
    2
  12-5-78
1357-1605
8,150.
9,830.
    0.005
    0.38
  120.0
   12-6-78
 1030-1252
 8,560.
10,3^0.
0.0335
0.0107
0.0442
0.0152
0.0075
0.0227
0.0241
0.0029
0.0270
     0.007
     0.48

    99.54
   120.0
1
 Based on Total Particulates captured by train.
e\                        _
 Standard Conditions =• 68 F and 29-92 inches mere ury

•^Opacfty results 1tsted are in minutes of the observed reading during the 120
 minute test period.
                                   - 28 -

-------
                         GEORGIA KAOLIN COMPANY
                          Dry Branch, Georgta

                                TABLE

                       PARTtCLE SIZE DISTRIBUTION
Date:    December 6, 1978
Location:  Georgia Kaolin
Sampling Location:  Raymond Mill
Traverse Point No. Sampled:    X~
                                              Pbar (In. HgO
                                              Stack Temp  ( F)
                                              Sample Time  (Min)
                                              Sample Volume  (cf)
                                              Moisture  (% H20)
                                              Meter Temp  (ฐF)
                                              Flow Setting,  H
                                                (in. H2)
                                              Nozzle Diameter  (in.)
                                                                    29.98
                                                                   135.
                                                                       946
 5
 2
 8.
82.
 0.94

 0.188
Sample Flow Rate  (at stack conditions):  0.59 cfm
Plate
No.
1
2
3
4
5;
6
7
8
Net.Wt.
(mg)
35.1
45.9
124.9
97-3
30.9
12.3
2.1
0.0
%
10.1
13-2
35.8
27.9
8.0
3-5
0.0
0.0
Cumulative
100.
89-9
76.7
40.9
13-0
0.6
0.0
EAD
(Microns)
13.1 and larger
8.1
5-5
3.8 •
1.2
0.7
ซ._..
Backup
 Filter
             0.0
                             0.0
                                              0.0
TOTAL
           348.5
                               -  29 -

-------
                                  RAYMOND  IMPACT MILL BAGHOUSE EXHAUST  STACK
                                       PARTICLE SIZE DISTRIBUTION
o
 I
EFFECTIVE AERODYNAMIC PARTICLE DIAMETER, microns
O O O O O O O OO— ' N> V*> -p- VI ON ซ-J 00 U) O
— K> V*> JT ui CT\ -vj OCAO O O O OOOOOOO
„


































































s
















/















/
s















x

















/
















•
/
















/

















/
















•

















/
















/















j
/•














t
jf
'















' .




































































































1





                 0.0!   O.C5 0. I 0.2 0.5  I
 10    20   30  40  50  60  70  80    90
      CUMULATIVE PERCENTAGE
(%  WEIGHT  LESS  THAN DIAMETER)

            FIGURE 7
                                                                                   95
                                         91  99
                                                                                                 98.1 99.9
                                                                                                            99.99

-------
                         GEORGIA KAOUN COMPANY
                          Dry Branch, Georgia

                                TABLE  10

                       PARTICLE SIZE DISTRIBUTION
Date:           December 6, 1978
Location:       Georgia Kaolin
Sampling Location: Roller Mill
Traverse Point No. Sampled:    Y-6
                                   Pbar  tln-  H9-*         29'98
                                   Stack Temp (ฐF)       135.
                                   Sample Time  (Min)       3.
                                   Sample Volume  (cf)      2.796
                                   Moisture  (%  H20)        8.
                                   Reter Temp (ฐF)        96.
                                   Flow Setting,  H        2.6
                                      (in. H2)
                                   Nozzle Diameter  (in.)   0.188
Sample Flow Rate (at stack conditions):
Plate
No.
1
2
3
4
5;
6
7
8
Net Wt.
(mg)
17.0
21. k
37.1
23.0
16.8
7-1
O.k
0.0 "."}
%
13.2
21.3
28.8
17.9
13.0
5.5
0.3
0.0
Cumulative
%
100
86.8
65.5
36.7
18.8
5.8
0.3
0.0
EAD
(Microns)
10.3 and larger
6.7
k.k
2.9
1.8
1.0
0.6
0.4
Backup
 Filter
  0.0
0.0
0.0
TOTAL
128.8
                             - 31 -

-------
                 ROLLER MILLS  BAQHOUSE EXHAUST  STACK
                      PARTICLE SIZE DISTRIBUTION
- Zฃ -
EFFECTIVE AERODYNAMIC PARTICLE DIAMETER, microns
o o ooooooo— .to oj-p-vnON^j covo o
— M >jj jr VI 
-------
             December 5,  1978
Date:
Type oT~tfischarge:   Stack
          Table II
 SUMMARY  OF  VISIBLE EMISSIONS

	 • Type of Plant:
Clay
Height of Point of Discharge: Approx!00'
Wind Direction:            Easi
Color of Plume: \~"~"
Observer No.:
                    wn i te
               Location of Discharge:Roller Mill  Outlet
               Description of Sky;   Clear Blue
               Wind Velocity:
               Detached Plume:"
                                                                   - iu mi/nr
                                                                Yes
Distance from Observer to Discharge Point: _
Direction of Observer from Discharge Point:
Height of Observation Point:    Approx.   100'
Description of Background:      Clear Blue
                                               Duration of  Observation:
                                             Approx. 25'	
                                         Approx.  2 n
                                                        Southeast
•
Set
Number
1
2
3
k
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
SUMMARY OF AVERAGE OPACITY
Tl
Start
0953
0958
1003
1008
1013
1018
1023
1028
1033
1044
1049
1054
1059
1104
1109
1114
1119
1124
1129
1134
Tie
End
0958
1003
1008
1013
1018
1023
1028
1033
1038
1049
1054
1059
1104
1109
1114
1119
1124
1129
1134
1139
Op<
Sum
100
90
95
100
90
100
90
100
55
100
95
100
100
100
100
95
100
90
100
100
aclty
Average
5
5
5
5 •
5
5
5"
5
2.9
5
5
5
5
5
5
5
5
5 .
5
5
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
T
Start
1139
1144
1149
1154
1159















me
End
1144
1149
1154
1159
1203
















Opa
Sum
95
95
80 .
95
70















pity
Average
5
5
4.7
5
4.4















Sketch Showing How Opacity Varied with Time:

              10,	:	
 Opacity
   (*)
                                       ™
                                 lo
                                                   V hr
                                                 Time .,
                            TT
                    2'.hr
                                            -33-

-------
           December 1978.
Date:       	
Type of Discharge:   Stack
          Table 12
 SUMMARY  OF  VISIBLE EMISSIONS

	 •  Type of Plant:
Height of Po.int of Discharge:
Wind Direction: _   East
Color of Plume: _
Observer No.:
                                Approx.  100'
                     White
Distance from Observer to Discharge Point:	
Direction of Observer from Discharge Point:  Southeast
Height of Observation PoTnt; 	
Description of Background: 	
               Description of Sky:
               Wind Velocity:
               Detached Plume:
               Duration of Observation:
              Approx.   25'
Clay
charge:
Sky:
5 -
Ro 1 1 e r Mill
Clear Blue
10 mi/h
Outlet


Yes
                                                                            Approx.  2  h
                                           Approx. 100'
                                           Clear Blue

Set
Number
1
2
3
k
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
SUMMARY OF AVERAGE OPACITY
Tl
Start
1050
1055
1105
1110
1115
1120
1125
1130
1135
1140
1145
1150
1155
1200
1205
1210
1215
1220
1225
1230
me
End
1055
1100
1110
1115
1120
1125
1130
1135
1140
1145
1150
1155
1200
1205
1210
1215
1220
1225
1230
•1235
•Opacity
Sum
0
0
'0
0
0
0
0 •
0
0
0
0
0
0
0
0
0
0
0
0
0
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Set
Number
21
22
23
2k
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
ko
T
Start
1235
1240
1245
1250
















me
End
1240
1245
1250
1251

















Opa
Sum
0
0
0 .
0
















pity
Average
0
0
0
0
















Sketch Showing How Opacity Varied with Time:

             10	
 Opacity
                                                  1 hr
                                                 Time .
                                                                    lo"
                                                       2  hr
                                           -34-

-------
          December 5,  1978
                         Stack
Date:     	
Type of Discharge:
Height of Pojnt of Discharge:
Wind Direction:	East
Color of Plume:
Observer No.:
           Table 13
 SUMMARY  OF  VISIBLE EMISSIONS

	 •  Type of Plant:
                                                                       Clay
                                100'
                      White
               Location  of Discharge;  Roller Mill  Outlet
               Description of Sky;   Clear Blue	
               Wind  Velocity:      5-10 mi/h	
               Detached  Plume:
 Yes
Distance from Observer to Discharge Point:         	
Direction of Observer from Discharge Point;"Southeast
Height of Observation Potnt; 	    100'
Descrlptton of Background: 	
               Duration  of Observation:
                    25'
                                                                          ^28t
                                       Clear Blue
-
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
SUMMARY OF AVERAGE OPACITY
Tl
Start
1357
1402
1407
1412
1417
1422
1427
1432
1437
1442
1447
1452
1457
1502
1507
1512
1517
1522
1527
1532
ne
End
1402
1407
1412
1417
1422
1427
1432
1437
1442
1447
1452
1457
1502
1507
1512
1517
1522
1527
1532
1537
Opacity
Sum
0
0
'0
0
0
0
0 •
0
0
0
0
0
0
0
0
0
0
0
0
0
Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
T
Start
1537
1542
1547
1552
1557
1602














me
End
1542
1547
1552
1557
1602
1605















Opa<
Sum
0
0
0 .
0
0
0














pity
Average
0
0
0
0
0
0














Sketch Showing How Opacity Varied with Time:

             10	
 Opacity
  (ซ
                       TT
                                                   1  h'r
                                                 Time
                            15
30
45
2.hr
                                           -35-

-------
                                       Table. 14
                                SUMMARY OF VISIBLE  EMISSIONS
             December 6, 1978
Date:
Type of Discharge:   Stack
Height of Po.int of Discharge;  Approx.  80'
Wind Direction:     Northwest  	
Color of Plume: 	
Observer No.:
wn i te
Distance from Observer to Discharge Point:
Direction of Observer from Discharge Point:
Height of Observation Potnt;
Descrlptton of Background:
                  Type of Plant:
                    Clay  Processing
Location of Discharge:
Description of Sky;     Blue
Wind Velocity:
Detached Plume:
                                            #8 Raymond Impact Mil 1
                                             5 mi/h
                  Duration of Observation:
                     7'
                      South
                           80T
    lireen nne  Forest
                                                   No
                                   1 1/2 h

Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
SUMMARY OF AVERAGE OPACITY
Tl
Start
1400
1405
1410
1415
1420
1425
1430
1435
1440
1445
1450
1455
1500
1505
1510
1515
1520
1525


ne
End
1405
1410
1415
1420
1425
1430
1435
1440
1445
1^50
1455
1500
1505
1510
1515
1520
1525
1530


Opacity
Sum
0
0
0
0
0
0
0
0
0
0
0
0
0
0
.0
0
0
0


Average
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0


Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
ko
T
Start




















me
End





















Opa
Sum




















fity
Average




















Sketch Showing How Opacity Varied with Time:
              10
 Opacity
  (ซ

1

15 '
0

30 45 V hr 15 3'0 <+5
Time , : .. .

2 hr

                                          -36-

-------
 APPENDIX A




RAW TEST DATA

-------
                     TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
PLANT   (^gOf^) C^    JCCXAhv^
nซ-rr     I*N  LJ ซ—^ TV
DATE
SAMPLING LOCATION
INSIDE OF FAR WALL TO
   OUTSIDE OF  PORT. (DISTANCE A> _
INSIDE OF NEAR WALL TO
   OUTSIDE OF  PORT. (DISTANCE B) •_
STACK I.D.. (DISTANCE A - DISTANCE B).
NEAREST UPSTREAM DISTURBANCE	
NEAREST DOWNSTREAMDISTURBANCE.
CALCULATOR.
                               3
                                                                          O

                                                                          o
                                                                  SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
x-y /
1 2
J3
V
5"
(,



FRACTION
OF STACK I.D.
.OW
./46
.1%
. -JSiV
.^s-y
,."7r

4-


















TRAVERSE POINT LOCA", ION
FROM OUTSIDE OF PORT
(SUM OF COLUMNS 4 & 5)
y7^
S"^
/2''
Jt"
3*V#*
.?vy**



















-------
                           PRELIMINARY VELOCITY TRAVERSE
PLANT
DATE
LOCATION   -^

STACK I.D.   3g? "
BAROMETRIC PRESSURE, in. Hg_

STACK GAUGE PRESSURE, in. H^O
            y . S*\ s\ A  t t
OPERATORS.
                           ฑjLฃ%._
                                                        SCHEMATIC OF TRAVERSE POINT LAYOUT
TRAVERSE
POINT
NUMBER
y- 1
j
:?
y
r
c








h









AVERAGE
VELOCITY
HEAD
Ups), in.H20
S.ZO
/.30
fo
/•So
j.^o
/.in


















/,%$
STACK
TEMPERATURE
(Ts), ฐF
S23
11}
y^v
/AT
/a
/. 35"


















t.&
STACK
TEMPERATURE
(Ts). 8F
te.3
/j r
;3 s-
>^rr
XJV


















/^f

-------
                      NOMOGRAPH DATA
PLANT.
DATE_
SAMPLING LOCATION
CONTROL BOX NO.  _
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT + 20 ฐF). "F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. Hg
(Pmฑ0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD. in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCED, in. H20
•^Hfa
Tmavg.
Bwo
pm
ps
p'pm
savg.
^pavg.
APmax.
t
•:/
./*
/,6
A 88
?o
W


/,*o
i*r
I.3&
l,6o
06
r55
5
0'

-------
PLANT
DATE
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER
OPERATOR
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE. (P,
FILTER NUMBER Is)
                                                                                                        5
                                                               PROBE LENGTH AND TYPE
                                                               NOZZLE I D._.  	  .
                                                               ASSUMED MOISTURE,'.	
                                                               SAMPLE BOX NUMBER	
                                                               METER BOX NUMBER	
                                                               METER AHfe	"*••*
                                                               C FACTOR	. 	tf'Ob.	
                                                               PI TOT  TUBE FACTOR     /f 3 ?
                                                                                      REFERENCE
                                                                                      NOTE
                                                                                                         /,
                                                 READ AND RECORD ALL DATA EVERY.
                                                                MINUTES
TRAVERSE
 POINT
 NUMBER
                 CLOCK TIME
__#7ฃ
             GAS METER READING
                           VELOCITY
                            HEAD
                          UP$I. in. H?0
                                                    68
ORIFICE PRESSURE
 DIFFERENTIAL
  (AH), in. H^O)
                                                           DESIRED  ACTUAL
                                                            .63
                                                                   3L
                                                                    .*<*
   STACK
TEMPERATURE
  (T$l."F
                                                                            /f z_
DRY GAS METER
TEMPERATURE
                                                                                        INLET    OUTLET
                                                                      to
                                                                        6
                                                                      TO
                                                                                                               -  -'•
                                                                                                                "
                                                                                                       <  „  U
                                                                                                       ^  J^
                                                                                                                  '0/9894
                                                                                                                    0.83"$
                                                                                                                  283575
                                                                                                         4&459J9&47
                                                                                                        1--* -
                                                                                                                                      i
                                                                                                                                      Tt
                                                                                                                    6P
                                                                                                                               if i i^OVi.

-------
                                                  ncuu DA^^
PLANT
DATE
SAMPLING LOCAT|Oj)
SAMPLE TYPE
RUN NUMBER
OPERATOR _
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE.!!?^
FILTER NUMBER M,'
 PROBE LENGTH AND TYPE
 NOZZLE 1.0. _.	  .
 ASSUMED MOISTURE.'.	
 SAMPLE BOX NUMBER	
 METER BOX NUMBER	
.METER AH,.	
 C FACTOR		
 PI TOT TUBE FACTOR
 REFERENCE -
 NOTE
                                   READ AND RECORD ALL DATA EV,ฃJปY

-------
                    TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
 PLANT
 DATE .
 SAMPLING LOCATION
 INSIDE OF FAR WALL TO
    OUTSIDE OF PORT. (DISTANCE A) _
 INSIDE OF NEAR WALL TO
    OUTSIDE OF PORT. (DISTANCE B! _
 STACK I.D.. (DISTANCE A  - DISTANCE B)
"NEAREST UPSTREAM DISTURBANCE	
 NEAREST DOWNSTREAM DISTURBANCE.
 CALCULATOR.
                                                                  SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
  POINT
 NUMBER
                 FRACTION
                OF STACK I.D.
STACK I.D.
    PRODUCT OF
  COLUMNS 2 AND 3
(TO NEAREST 1 8 INCH)
DISTANCE B
TRAVERSE POINT LOCA', ION
 FROM OUTSIDE OF PORT
 (SUM OF COLUMNS 4 & 5)
 -7   /
                                                                      3
      3
      9
      7
      9

                                                                    V

-------
                           PRELIMINARY VELOCITY TRAVERSE
PLANT.
DATE /J
LOCATION
STACK I.D..
BAROMETRIC PRESSURE, in. Hg      1.0.8?
STACK GAUGE PRESSURE, in. H20
OPERATORS
        \,
   TRAVERSE
     POINT
    NUMBER
       J
      /o
   AVERAGE
 VELOCITY
   HEAD
Ups). in.H20
                    Id)
                2 IT
                I.D
                 /f
   STACK
TEMPERATURE
  (Ts). eF
                 a 7
                                                       SCHEMATIC OF TRAVERSE POINT LAYOUT
,UปW (. I
TRAVERSE
  POINT
  NUMBER
                                                      y-
                                                          r
                                           7
                                          Sc?
                                                        y r*
                                       AVERAGE
VELOCITY
  HEAD
                                                                   /. 5*0
                                                    /, S"
                                                                    .O
                                                                  J.I3
                                                                  J.JF
  STACK
TEMPERATURE
   (Tsi. ฐF
                                                                  /,
                                                                                l.l  )

-------
                       NOMOGRAPH DATA
PLANT   <5"=i .




DATE._
                    ivx
         \-L- A-
SAMPLING LOCATION



CONTROL BOX NO. _
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE lAMBIENT + 20ฐF).ฐF
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. Hg
(Pmฑ0.073 x STACK GAUGE PRESSURE in in. H20)
U /
r,
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD. in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap. in. H20
^ ,
T(navg.
Bwo
pn,
ps
PsPm
savg.
t
Apavg.
APmax.
1 t
' '*ป
3C ,
/
V >^^
%
ซ
^o.o
So.i
1 - 0
I3o
\,15
2-. 3
??
^4
90
&6

-------
SAMPLING
SAMPLE
RUN NUMBER
OPERATOR
AMBIENT TEMPER AJURE
BAROMETRIC PRESSURE
STATIC PRESSURE. (Psl
FILTER NUMBER Is)
 Tent* ----
ffiwt Alt*
PROBE LENGTH AND TYPE"
NOZZLE I.D.y   JT^
ASSUMED MOISTURE.'. _งL. __.
SAMPLE BOX NUMBER
METER BOX NUMBER
METER AH.. V.g-y
C FACTOR
                                                                    7
                                                      PITOT TUBE FACTOR
                                                      REFERENCE 6p  /
            READ AND RECORD ALL DATA EVERY

-------

-------
                                                         DAW
SAMPLING LOCATION *
SAMPLE TYPE
RUN NUMBER
OPERATOR _
AMBIENT TEMPERAJURE
BAROMETRIC PRESSURE
STATIC PRESSURE.
FILTER NUMBER (s)
                             PROBE LENGTH ANDTYPE.
                             NOZZLE f D. ^ / W
                             ASSUMED MOISTURE.'.
                             SAMPLE BOX NUMBER
                             METER BOX NUMBER.
                             .METER AHb
                             C FACTOR
                             PITOT  TUBE FACTOR
                             REFERENCE
                             NOTE
READ AND RECORD ALL DATA EVERY
                     -.
                _3LtLL
                                                                        MINUTES
                                                                                DRY GAS METER
                                                                                TEMPERATURE
ORIFICE PRESSURE
  DIFFERENTIAL
  IAH). in. HjOl

-------
TRAVERSE
 POINT
 NUMBER
                 CLOCK TIME
CAS METER READING
    IVI. II3
 VELOCITY
  HEAD
mp$>. in HjQ
ORIFICE PRESSURE
 DIFFERENTIAL
  IAH). in HOl
                                                         DESIRED ACTUAL
   STACK
TEMPERATURE
  lTfl.ฐF
DRY GAS METER
TEMPERATURE
                                                                                    INLET   OUTLET
 PUMP
VACUUM.
 in HI
 SAMPLE BOX
TEMPERATURE.
     ฐF
  1 (WINGER
TEMPERATURE.
     ฐF
y-;
T-air.v
                                                         /vr
                                   11L
                                                                      3L
                                                         X99
                                                                                                                        ฅ2-
                                                                                   &-
                                                                                   &-
   0
  T^:
                                                                                      '
                                                                                             y

-------
                                 SUMMARY
                      RECORD  OF  VISIBLE  EMISSIONS
Type of Plant    (  7  (r-a,.	     Observer
                  /       	jr  w -...	
Type of Discharge V^TAC^/   OTHER

Discharge Location
Height of Point-of Discharge 	21

Observer's Location:
                                       /
    Distance to Discharge Point   •  7
    Height of Observation Point     ^ '
    Direction from Discharge Point

Background Description 	(
                   Overcast '   Partly Cloudy    Other       ,  Sky Color
                                          f
          VJind Direction     A/  a/  	  Wind Velocity         -5"    mi/hr

Plume Description:

    Detached:  Yes

    Color:  Black   (T/hit
-------
                            RECORD OF VISIBLE EMISSIONS
Company Name   (r
o
0
0
o
o
o
o
o
o
0
0
o
o
COMMEOTS









,



1
_i
f
i




i
i
i
•








-------
                         RECORD OK VISIBLE EMISSIONS



Company Name    G-3 . K
0
0
o
30
o
0
o
V
o
ti
o
o
o
&
o
Q
o
0
o
o
o
o
0
0
o
o
6>
O
o
0
0
C3
o
0
45
o
Q

-------
       RECORD OF VISIBLE EMISSIONS
•  ซ &o \ > /$._• _    Date __
Company flame
Plant Address    "Dwyy f^v-oxe-k . G&..
                      /             -1
Stack Location 	?  ft
                                                              &OP
                                                Observer
Weather Conditions   See  V-gce>voC
                                                Observer's
                                                 Location
TIME
HR

/S




























/5
MIN

00
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
/19
20
21
22
23
24
25
26
27
28
29
SECONDS
00
o
o
o
0
o
o
o
o
c
G/
O
0
o
0
o
o
o
&
o
0
o
o
o
o
•o
o
&
0
o
o
15
o
a
o
o
0
o
o
o
a
o
O
o
o
0
c?
&>
0
c?
0
o
o
o
o
o
O
0
0
o
o
o
30
o
o
o
e>
O
0
o
o
o
0
o
o
o
o
o
o
o
o
o
o
ฃป
c>
o
o
o
o
o
o
0
o

45
O
o
&
O
o
o>
o
o
o
o
o
o
0
o
o
0
0
o
o
0
o
o
o
o
o
c>
&
o
o
o
COMMENTS









.



,
j
•
}




\
i

i

•






-------
PLANT

-------
TRAVERSE
 POINT
 NUMBER
                 CLOCK TIME
                           GAS METER READING
                               .VBi. II3
                                     VELOCITY
                                       HEAD
                                    (Ap$l. in. H^O
ORIFICE PRESSURE
 DIFFERENTIAL
  (AH), in H?0i
                                               DESIRED  ACTUAL
   STACK
TEMPERATURE
  (T$I.ฐF
DRY GAS METER
TEMPERATURE
                                                                                    INLET
                                                                                   ซT.JB..-F
                                                                                         OUTLET
                                                                                        
-------
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
PLANT	
DATE	
SAMPLING LOCATION
INSIDE OF FAR WALL TO
 .  OUTSIDE  OF PORT. (DISTANCE A) _
INSIDE OF NEAR WALL TO
   OUTSIDE  OF PORT. (DISTANCE B) _
STACK I.D.. (DISTANCE A - DISTANCE B).
NEAREST UPSTREAM DISTURBANCE	
NEAREST DOWNSTREAM DJSTURBANCE _
CALCULATOR
              17
                          /ปฃ•? P.p.
                                             SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
X- /
IT
3
4
^r
6
7
e
f
/o
ft
12
f?
^










FRACTION
OF STACK I.D.
,0(?
.os-i
.a'*'}
,1-tt
,-LoJ
, 1^=5
,-iU
.4S-V
.1^1
.T^^
. *5*
,^01
.9-V?
.•5?^-
' ซ









STACK I.D.
1 7 . V7 S























PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1 8 INCH)
" y^
\
i V^
2 XL
3 'A.
^ VJP
4 V^
Tป
irV-v
\^ v^
lA^
i r#i
R V^
u %







\


DISTANCE B
SV^f<























TRAVERSE POINT LOCA^, ION
FROM OUTSIDE OF PORT
(SUM OF COLUMNS 4 & 5)
SV4 "
UA
7
n V4
7V^
? 7/a
- I I */8
\ (, '/4
\t>
\5 '/a
lO'/fl
TO r/8
*.v*/ft
T-T'/S









,

-------
PRELIMINARY VELOCITY TRAVERSE
PLANT C-7* , K3hto ^ป-v
DATE I T-- 
13 L
13*7
/57
J37
/ฃ7
/3&
/3 ?
/**
/3%
ft*
/3&
/3€
f ^f*) cS








/ &\ ^^
i
                          SCHEMATIC OF TRAVERSE POINT LAYOUT
                        TRAVERSE
                          POINT
                          NUMBER
                          AVERAGE
VELOCITY
  HEAD
IAps>. i
                                      A75"
  STACK
TEMPERATURE
   (Tsป. ฐF
                                                   /3S
                                                 S42.
               fit-

-------
                      NOMOGRAPH DATA
PLANT




DATE_
SAMPLING LOCATION



CONTROL BOX NO.  _
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE ( AMBIENT + 20 ฐF),ฐF
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. Hg -.-^ ( j
(Pmฑ0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD. in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR I
CALCULATED NOZZLE DIAMETER, in.
/
ACTUAL NOZZLE DIAMETER, in.
REFERENCE Ap. in. H20
^HCa
T|navg.
Bwo
pm
PS
P'Pm
savg.
•*Pavg.
•^Pmax.
/.6
J\
.1
/.t
/,??
?o
7


/.o
/4o
/,**
2.2~o
)
it
99
~s~

-------
PLANT.
DATE_
SAMPLING LOCATION.
SAMPLE TYPE	
RUN NUMBER.
OPERATOR.
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE .
STATIC PRESSURE. |P$)_
FILTER NUMBER (s)	
                        .- S .  J
                            fJt^S; < tf
 PROBE LENGTH AND TYPE.
 NOZZLE ID...	*l(
 ASSUMED MOISTURE.".	
 SAMPLE BOX NUMBER	
 METER BOX NUMBER.
• METER AHto	
 C FACTOR	.  .  ,
 PI TOT TUBE FACTOR
 REFERENCE Ap	L
 NOTE 	
                                  READ AND RECORD ALL DATA EVERY.
                                                                     MINUTES
                                                                             DRY GAS METER
                                                                             TEMPERATURE
                                              ORIFICE PRESSURE
                                               DIFFERENTIAL
                                                IAH). in. HJDl
                                                                                                                        ;^>*1^:;pฃ
                                                                                                                        •; •. ,-  •ปif,f ix!;--':-1
                                                                   Ul	IM

-------
TRAVERSE
 POINT
 NUMBER
                    CLOCK TIME
                       GAS METER READING
 VELOCITY
   HEAD
Uipl  m H0
ORIFICE PRESSURE
  DIFFERENTIAL
  IdHh in HjO)
                                                                     DESIRED   ACTUAL
   STACK
TEMPERATURE
  iT$i.ฐF
DRY GAS METER
TEMPERATURE
                                                                                                      INLET    OUTLET
 PUMP
VACUUM.
 in  H|
 SAMPLE BOX
TEMPERATURE.
  IMPINGER
TEMPERATURE
      ฐF
Tn,
      A
i

-------
PLANT.
DATEL
SAMPLING LOCATION
SAMPLE TYPE  <
RUN NUMBER:
OPERATOR :__
AMBIENT .TEMPERATURE	ฃ1
BAROMETRIC PRESSUR^   "?.
STATIC PRESSURE. 
-------
                   TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
     he.

PLANT
DATE ...19,.
SAMPLING LOCATION _
INSIDE OF FAR WALL TO
   OUTSIDE  OF PORT, (DISTANCE A) _
INSIDE OF NEAR WALL TO
   OUTSIDE  OF PORT. (DISTANCE B) _
STACK I.D.. (DISTANCE A • DISTANCE B).
NEAREST UPSTREAM DISTURBANCE	
NEAREST DOWNSTREAM DISTURBANCE.
CALCULATOR.
            fecy Q IV
                                       •'  \\
                                 St."
                                                                 SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
  POINT
 NUMBER
 FRACTION
OF STACK I.D.
                               STACK I.D.
    PRODUCT OF
  COLUMNS 2 AND 1
(TO NEAREST I 8 INCH)
DISTANCE B
TRAVERSE POINT LOCA'i ION
 FROM OUTSIDE OF PORT
 (SUM OF COLUMNS 4 & 5)


      ฑ.
                                                                          SL
                                                                                     <*>
-------
       PRELIMINARY VELOCITY TRAVERSE
''
PLANT     V3 fr .  V
DATE	Ull
LOCATION    I€.-B\\
STACK I.D.	}
BAROMETRIC PRESSURE, in.                	
STACK GAUGE PRESSURE, in. H.Q    - .  0 "7
OPERATORS      5 a^^a>v    Q * fJ 7
STACK
TEMPERATURE
(Ts>. 8F



















































TRAVERSE
POINT
NUMBER
V- i
1
T,
^
^
k
1
I




V ' '











AVERAGE
VELOCITY
HEAD
Qpsi, in.H20
i '
.V\5"
. \4
^
. >^S
. \^
• ^
.\^^
















, /3/
STACK
TEMPERATURE
(Tsi. ฐF








-






'










-------
                    NOMOGRAPH DATA
PLANT.
DATE._
SAMPLING LOCATION
CONTROL BOX NO. _
CALIBRATED PRESSURE DIFFERENTIAL ACROSS
ORIFICE, in. H20
AVERAGE METER TEMPERATURE (AMBIENT 4- 20 ฐF), "F
PERCENT MOISTURE IN GAS STREAM BY VOLUME
BAROMETRIC PRESSURE AT METER, in Hg
STATIC PRESSURE IN STACK, in. Hg - . 0 "7
(Pmฑ0.073 x STACK GAUGE PRESSURE in in. H20)
RATIO OF STATIC PRESSURE TO METER PRESSURE
AVERAGE STACK TEMPERATURE, ฐF
AVERAGE VELOCITY HEAD. in. H20
MAXIMUM VELOCITY HEAD. in. H20
C FACTOR
CALCULATED NOZZLE DIAMETER, in.
APTIIfil Mn77l C nifiMPTCR in
<\\i 1 UHL nUฃฃLll UIHIilL 1 Cn. In.
REFERENCE Ap. in. H20
^
T(navi.
Bwo
pm
ps
Ps?m
savg.
•^pavg.
APmax.

,*f
JL,1
•-T7/
-err
/.9
90
.&$%
i3.W>
—
s.o
-rf
^^
^
>\
$ J5?
^-y ป5>}J
"3* ,100
n*
                                           I.M5

-------
PLANT
DATE
SAMPLING LOCATI
SAMPLE TYPE
RUN NUMBER
OPERATOR
AMBIENT TEMPERAJURE
BAROMETRIC PRESSURE
STATIC PRESSURE. fPs>
FILTER NUMBER Is)
     PROBE LENGTH ANOJJP,
     NOZZLE ID..   ป
     ASSUMED MOISTURE. % _
     SAMPLE BOX NUMBER __l
     METER BOX NUMBER
    .METER „..„	=
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     30
     31
     32
     33
     34
     35
     36
     37
     38
     39
     40
     41
     42
     43
     44
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     47
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     50
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MIN

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01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
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20
21
22
23
24
25
26
27
28
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31
32
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20
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10
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10
11
12
13
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04
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08
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10
11
12
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14
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20
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-------
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Company Name
Plant Address _/0'
Stack Location
RECORD OF VISIBLE EMISSIONS
          I          Date _
                                                       / 3-6-
                                                          ________
                     hYt nc \\  Qgfl.    Observer    J  < D . ft 'ฃ)& ,'//
Weather Conditions
                         Hi/I
                    Observer's
                     Location
TIME
HR

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Company flame

Plant Address
  RECORD OF VISIBLE  EMISSIONS

ฃ  ifc&tsl^	    Date
Stack Location
                       Observer
Weather Conditions
                       Observer's
                        Location

HR

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WIN

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-------
    APPENDIX B




LABORATORY REPORTS

-------
                                     ANALYTICAL DATA
PLANT	

DATE.	J^L

SAMPLING LOCATION	

SAMPLE TYPE 	\

RUN NUMBER	
SAMPLE BOX NUMBER

CLEAN UP MAN	
                         K
                                                COMMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE. PROBE, CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                 1AA-1O
                           LABORATORY RESULTS

CONTAINER RI NI> \ ft    ^OH \S
                                                                          3j 5*73 .
                                                FRONT HALF SUBTOTAL
                                                                                          m,
                                                                                         .mg
                                                                                         . mg
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS, AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS,
    AND BACK HALF OF FILTER HOLDER
ETHER-CHLOROFORM
EXTRA^TinN

BACK HALF SUBTOTAL

TOTAL WFIGHT SV6

mg
mg
mg

+**\ "18

MOISTURE

  IMPINGERS
   FINAL VOLUME   "2-^ ฐ
   INITIAL VOLUME	^Q0
   NET VOLUME   _
  SILICA GEL
   FINAL WEIGHT
   INITIAL WEIGHT
   NET WEIGHT
                        ml
                        ml
                                                            TOTAL MOISTURE
                              SUBTOTAL

-------
                                   ANALYTICAL DATA
PLANT_
-------
                                   ANALYTICAL DATA
SAMPLING LOCATION

SAMPLE TYPE

RUN NUMBER.

SAMPLE BOX NUMBER

CLEAN UP MAN
                              O
                                              COMMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                                                                        LABORATORY RESULTS
                                              CONTAINER


                                              CONTAINER
                                              FRONT HALF SUBTOTAL
                                                                        S3-7
                                                                                     .mg
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS. AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS.
    AND BACK HALF OF FILTER HOLDER
MOISTURE
IMPINGERS
FINAL VOLUME _
INITIAL VOLUME <
NET VOLUME _
SILICA GEL
FINAL WEIGHT <•
INITIAL WEIGHT .ฃ
NET WEIGHT
^^L.ml
*a& mi
S & Q m'
2/-?.o g
,?oo f
/^ .
                                             CONTAINER	
                                             ETHER-CHLOROFORM
                                               EXTRACTION
                                              BACK HALF SUBTOTAL
                                                         TOTAL MOISTURE
.mg

.mg

.mg

TOTAL WEIGHT
S-3 .-7

mg

                             SUBTOTAL

-------
                                    ANALYTICAL DATA
 PLANT J
 DATE
 SAMPLING LOCATION
 SAMPLE TYPE
RUN NUMBER  <3 A
SAMPLE BOX NUMBER  V
CLEAN UP MAN
COMMENTS:
FRONT HALF
  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
CONTAINER

CONTAINER
.^ A
                           LABORATORY RESULTS
                                         me
FRONT HALF SUBTOTAL   7 I'U
                                                                                        ,mg
                                                                                       .mg
BACK HALF
  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS. AND BACK
    HALF OF FILTER HOLDER
ACETONE WASH OF IMPINGERS. CONNECTORS.
    AND BACK HALF OF FILTER HOLDER
MOISTURE
IMPINGERS
FINAL VOLUME j
INITIAL VOLUME j
NET VOLUME _
SILICA GEL
FINAL WEIGHT .
INITIAL WEIGHT j
NET WEIGHT
of / j ml
•3?<90 ml
•5*5" ml
y)r
ฃซ!9sJ g
./^"•S"" g -- 	
g
g
-t
                                     'i. r
ETHER-CHLOROFORM
EXTRACTION
CONTAINER
BACK HALF SUBTOTAL
mg
mg
fllg

TOTAL WF'GHT ? f ป> ft

mg

                                                           TOTAL MOISTURE.
                             SU8TOIAL

-------
                                     ANALYTICAL DATA
 PLANT	ฅ2

 DATE _  .

 SAMPLING LOCATION .

 SAMPLE TYPE  	

 RUN NUMBER	

 SAMPLE BOX NUMBER
CLEAN UP MAN	
COMMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER  _^
                           LABORATORY RESULTS

CONTAINERRTStฑ\P      1 ft ฐ\\ > 3  m.


CONTAINER ftKT^*' ff       0 Jt5  > 3  mg
                                                FRONT HALF SUBTOTAL
                                         .nig
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS. AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS.
    AND BACK HALF OF FILTER HOLDER
MOISTURE

  IMPINGERS           ^
   FINAL VOLUME   <*7?  ml
   INITIAL VOLUME  *2%>  ml
   NET VOLUME       V> ml
  SILICA GEL
   FINAL WEIGHT
   INITIAL WEIGHT
   NET WEIGHT
ETHER-CHLOROFORM
FXTPACTin"
CONTAINER
BACK HALF SUBTOTAL
mg
mg
me

TOTAI *FIRHT Hfi^^

A *

            TOTAL MOISTURE
                              SUBTOTAL

-------
                                    ANALYTICAL DATA
PLANT_ C

DATE_

SAMPLING LOCATION

SAMPLE TYPE  f t

RUNNUMBLR_
              O t^J
SAMPLE BOX NUMBER 3u_

CLEAN UP MAN.
                                               COMMENTS-
                    l  u \C~ trt
FRONT HALF                              -

  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDEF
  FILTER NUMBER  .s
                                              CONTAINER


                                              CONTAINER
                                                                        LABORATORY RESULTS
.mg
                                                                           33.?
                                              FRONT HALF SUBTOTAL
                                                                                      .mg
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS. AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS, CONNECTORS.
    AND BACK HALF OF FILTER HOLDER
                                              ETHER-CHLOROFORM
                                                EXTRACTION
                                              BACK HALF SUBTOTAL
                                               TOTAL WEIGHT
.mg

.mg

.mg

.mg
                                                                                       mj
MOISTURE

  IMPINGERS      ~  • ^
  .FINAL VOLUME  3  ' P  ml
   INITIAL VOLUME o?.P O  ml
   NET VOLUME    I  < 0  ml

  SILICA GEL      ^..  ฃT
   FINAL WEIGHT  ^(!oซ  g
   INITIAL WEIGHT 2ฎ**. I
   NET WEIGHT      /Q • J K
                                                          TOTAL MOISTURE
                             SUBTOTAL

-------
                                  ANALYTICAL DATA
PLANT.

DATE _

SAMPLING LOCATION

SAMPLE TYPE    1 Q,^

RUN NUMBLR  T\J O
                           vr.i\
                         J
SAMPLE BOX NUMBER
CLEAN UP MAN	(.


FRONT HALF
  ACETONE WASH OF NOZZLE. PROBE, CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                                             COMMENTS:
                                              /"/Vox
                                            CONTAINER
CONTA.NER
                                                                      LABORATORY RESULTS
                                                           -^ F
                                                                                   .ing
                                             FRONT HALF SUBTOTAL
                                                                       a.a.7
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS. AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS.
    AND BACK HALF OF FILTER HOLDER
MOISTURE
ETHER-CHLOROFORM
EXTRACTION
CONTAINER 	
BACK HALF SUBTOTAL
TOTAL YYPiGHT ซ^ซ*

mg
ing
mi
. ป \ mg

IMPINGERS ^ -^
FINAL VOLUME 3 -jD_ ml
INITIAI VniUMF 3-O^> ml
NF_TVnL"MF \ ^O ml
SILICA GEL oil U
FIN&L *Flf.HT &.ljtl g
INITIAL ^FI^.HT e^^ g
NET WEICrHT 1*3 'f g
S
g
g
{
UBTOTAL .
                                                        TOTAL MOISTURE,

-------
                                   ANALYTICAL DATA
PLANT _OCG.
OATE_.  1^.1 0:13
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER
                       v>   rVi I I
SAMPLE BOX NUMBER

CLEAN UP MAN _
                                             COMMENTS:
FRONT HALF

  ACETONE WASH OF NOZZLE. PROBE. CYCLONE (BYPASS).
    FLASK. FRONT HALF OF FILTER HOLDER
  FILTER NUMBER
                                             CONTAINER
                                                                      LABORATORY RESULTS
.mg
                                             FRONT HALF SUBTOTAL
                                                                        ^7 1 Q
                                                                                    .mg
                                                                                    .mg
BACK HALF

  IMPINGER CONTENTS AND WATER WASH OF
    IMPINGERS. CONNECTORS. AND BACK
    HALF OF FILTER HOLDER

ACETONE WASH OF IMPINGERS. CONNECTORS.
    AND BACK HALF OF FILTER HOLDER
MOISTURE
IMPINGERS ,
FINAL VOLUME e
INITIAL VOLUME _C
NET VOLUME
SILICA GEL
FINAL WEIGHT
INITIAL WEIGHT '
NET WEIGHT
ฑ35
sust*
35
a 13
SOD
V*
ml
ml
ml
g
g
I ,.
ETHER-CHLOROFORM
EXTRACTION
BACK HALF SUBTOTAL
TOTAL WEIGHT
mg
mg
mg

ฃ-7.0 ซ

                                                         TOTAL MOISTURE
                                                                         5ฃ
                            SUBTOTAL

-------
I  I
TITLE
 From Page No --
                                               Project No.
                                              _ Book No.
                        W
                                                     •73
                                                               ,/M
                                                   •m
                                                              ftvs
                                            Y$L
                                   \(K
                     id.
                                M-l
                          V./yfl
                                                   If
                               3^0
                                                                    OCOS
    -ZP
          ,
                                          'Z. /SYS"
                                                                    ซ56
                                                          .^/'
JJ^-
          fy
3S
                     /v-
                              c&'*L
Saw
         107
                                                            :


-------
I  I
 TITLE
"  rairTigle   S/'
                                    //g.
Project No.   '
  Book No	
                                                                                    - 4, ^ซ~.." -Jl-^ -X,.
                                                                                            12
From Pag* No..
  a,eai
          riHA.1

           CO
                                          Cz)
                       2

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                                         0.


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                                                              0./6/7
                                                              (?, /S0?
                                                               ). 203^r
                             0.0973


                             Q.6I23
                                                                                 To
 Witncsiod & Understood by me.
                               Date
                                           Invented by
                                                                         Dale
                                           Recorded by   *.*.,..

-------
                                             Project No.
                                              Book No.
                                                                             -13
                                '<&'
't'
                                        6.16515
                                        6, ft ii
                                                  0:<
-------
TITLE.
                                   No..
From Page No
                                (0


                                                                                      ..-.fr r ^ - .-.r.i >rRVi"ซ

                                                                                     ''
                                                          ~
      ; 7W 9xu<^
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                                                   0.H37/'
                  -2.4470
                       71
                                                      l.f fOf
                                                      2.S131
                                                      5.71***
    "^ •~', -
                                                                                   To
                                                                                      'age No..
 Witnessed & Understood by me.
Dale
 //-*•• 75
               Invented by
                                                                          Date
                                           Recorded by

-------


       j


•   t- /•  ~ J?-ป''5wป*
i& full"   dfoniKt-
                                                        • .iiliฃsfiiSS"!:

-------
     APPENDIX C




SAMPLE CALCULATIONS

-------
                                SAMPLE CALCULATIONS
Test Run  1   #8  Raymond  Impact Mill Exhaust Stack - 12-6-78
1.  Volume of dry gas sampled at standard conditions  (68ฐF,  29-92
    in. Hg), dscf.
    Vm(std)
                         17.647  x  Y  x  Vm   x    ( Pfa  +
                                        m
                                                                                  65.04
                          i/.OH/  x  u.yo*t   x oy.u/  x(  ty-yo  •>  —mr J
    V
                     17.647  x  0.984   x 69.07   x(
'm(std)           a   	
                                        (95.
    Where:     .  ..

    ^m(std)          ~   Volume of gas sample measured by the dry gas meter,
                         corrected to standard conditions, dscf.

    V                a   Volume of gas sample measured by the dry gas meter at
                         meter conditions, dcf.

    Pjj               a   Barometric pressure, in. Hg.

   &H               a   Average pressure drop across the orifice meter,
                         in. H20.

    T                a   Average dry gas meter temperature, ฐF.

    17-647           a   Factor that includes ratio of standard temperature
                         (528ฐR) to standard pressure (29-92 in. Hg)?ฐR/in. Hg.

    Y                a   Dry gas meter calibration factor.


2.  Volume of water vapor in the gas sample corrected to standard conditions, scf.

    Vw(std)          "  (0-0-707 x  Vwc) + (0.04715  x  W^

    Vw(stdj          -  (0.04707 x  90.01 +  CO.04715 x  14.5  1    = 4.92

    Where:

    Vw(std)          =   Volume of water vapor in the gas sample corrected to
                         standard conditions, scf.

    V                =   Volume of liquid condensed in impingers, ml.

-------
                                       - 2 -
     wsg

    0.04707
                     Weight of water vapor collected  in silica gel,  g.

                     Factor which includes the density of water
                     (0.002201 lb/ml), the molecular weight of water
                     (18.0 Ib/lb-mole), the  ideal gas constant
                     [21.85  Un. FfgJ  (ft3)/Ob-mole) (ฐR)]  . absolute
                     temperature at standard conditions  (528ฐR),  absolute
                     pressure at standard conditions  (29.92  in.  Hg), f
    0.04715
                     Factor which includes the molecular weight of water
                     (18.0 Ib/lb-mole), the ideal gas constant
                     [21.85 (in. Hg)(ft3)/(1b-mo1e)(ฐR)l7 absolute
                     temperature at standard conditions \528ฐR), absolute
                     pressure at standard conditions  (29.92  in. Hg), and
                     453.6 g/lb, ft3/g.
3.  Moisture content.
     ws
                                 w(std)
                      w(std)
                                        m(std)
     ws
    Where:
     ws
                                  4.92
                             k. 92  •*•  65.04
                                              = 0.070
                     Proportion of water vapor, by volume, in the gas
                     stream, dimension less.
4.   Mole fraction of dry gas.
    M
                     1 - B
                              ws
    M
                     1 - 0.070
              0.930
Where:


Md
                         Mole fraction of dry gas, dimensionless
5.   Dry molecular weight of gas stream, Ib/lb-mole.
    MW,
0.440(3C02)   +  0.320 (*02)  + Q.28Q
                                                                 +  % CO)

-------
                                       - 3 -


    MWd              =   (O.Mป0 x 0.3  )+  (0.320x21.3 ) -i-[o.280  (  0.0  +78.4   )]


                         28.97


    Where:

    MW,              ป   Dry molecular weight, Ib/lb-mole.


    $C02             ฐ   Percent carbon dixoide by volume, dry basis.


    %Qj              a   Percent oxygen by volume, dry basis.


    3>N_              ซ   Percent nitrogen by volume, dry basis.

    %CQ              m   Percent .carbon monoxide by volume, dry basis.

    O.Mป0            ป   Molecular weight of carbon dioxide, divided by  100.

    0.320            =   Molecular weight of oxygen, divided by 100.

    0.280            a   Molecular weight of nitrogen or carbon monoxide,
                         divided by 100.


6.   Actual molecular weight of gas stream (wet basis), Ib/lb-mole.

    MWs              -    (MWd  x' Md)   +   [18  (1 - Md)]


    MW               =(28.98x0.930)        + [18  (1  -0.930 )]

                     = 28.20

       <                                                                     ,
    Where:

    MW               =   Molecular weight of wet gas, Ib/lb-mole.

    18               ซป   Molecular weight of water,  Ib/lb-mole.


7-   Average velocity of gas stream at actual  conditions, ft/sec.
vs               -     85.^9x0
  5                             p
                                      x
                                                                '    r   ^   ^
                                                                 s  Cavg)
                                                              _
                                                              ~  *  M^

-------
                                       - 4 -


                          85.49   x  0.850 x  1.319 x

                           80.0

    Where:

                     ป   Average gas stream velocity, ft/sec.
                                                       f (131. + 460.^
                                                       [JO.09  x 28.20
    85-49            *   Pi tot tube constant, ft/sec  X

                        r(lb/lb-moTe)(ln.Hg)"U
                        L (ฐR) (in. H20)    j  '

    C                a   PJtot tube coefficient, dimensionless


   Ap               "Velocity head of stack gas, in ^0.

    T                =   Absolute  gas stream temperature,  R.

    P                •   Absolute gas stack pressure, in. Hg.


8.  Average gas stream dry volumetric flow rates, dscf/min.

                         1058.8   xir   xA   x  M.  x  P
                     '
    n
    Qs(std)

    o                    1058.8x80.0  x :  3.69  x 0.930 x 30.05
    V(std) -         *                (  131.  +  A60)

                     =  14790.

    Where:

    Q /   ,\          ป   Volumetric flow rate of dry stack gas, corrected to
        t                 standard conditions, dscf/min.
                                                          2
    A                =   Cross-sectional area of stack, ft .

    1058.8           =   Factor which includes standard temperature  (528ฐR) ,
                         standard pressure (29-92 in. Hg) , and 60 sec/min,
                         (ฐR) (sec)
                        (in. Hg)(min) '
9-  Isokinetic variation calculated from intermediate values, percent.

-------
                                       - 5 -

                         17'316  x  Ts   *  Vstd)

                         v   x  6  x  P   x  M.  x   (D  )2
                          s            son


                     -   17.316 x 591.  x  65.04
                          80.0   x  96.0 *  30.09X 0.930 *      .180  )

                     -    95.6

    Where:

    I                 =   Percent of isokinetic sampling.

    6                =•   Total sampling time, minutes.

    0                ป   Diameter of nozzle, inches.

    17.316           -   Factor which includes standard temperature  (528ฐR) ,
                         standard pressure (29-92 in. Hg) , the formula  for
                         calculating area of circle tf D*     ^^t  „„. .     f
                                   3                  i ••   , conversion of

                         square feet to square inches (  144), conversion of
                         seconds to minutes  (60), and conversion  to
                         percent (100), (in. Hg) (in2)  (min) .

                                        (ฐR) (ft2) (sec)


10.   Particulate concentration, gr/dscf.

    C,               ป   0.015^32 x M
                                    Vm(std)

    C]               -   0.015432  x   -jgL	    '

    Where:
        i
    C.               a   Particulate concentration, gr/dscf.

    M                ป   Total weight of particulate caught by train, mg.

    0.015^32         a   Conversion factor of gr/mg.


11.   Particulate mass emission rate, Ib/hr.

    PMRt             =   0.008571 k  x  C1  x  Qs(std)


                     =   0.0085714  x 0.020  x14,790   . 2.49

-------
                                   - 6 -
Where:

PMR              =   Participate mass emission rate,  Ib/hr.

0.0085714        *   Conversion factor relating minutes to hours  (60),  and
                     grains to pounds (7,000),(Ib)  (min)/(gr)  (hr).

-------
        APPENDIX D




EQUIPMENT CALIBRATION DATA

-------
                                                                          23
                                                                                 0-K.

                                                                               -. O.f.
     Date    ///31/79
     Barometric pressure, Pw =33-/J\n.  Mg
          Box  No.,

Ory gas meter  llo.
Orifice
manometer
setting,
All.
in. HjO
0.5
1.0
t.s-
4.o
3.o
8.0
Gas volume
wet test
meter
Vw,
ft3
5
5
S"
10
10
10
Gas volume
dry gas
meter
vdซ
ซ3
JS"7. 30?
d&3. SS~S
P.-.J. i-J-J
-3i7, V V-3
i67? T,;^
j •? 2 . ' 3 e
J$ <-f /i/o
^S-V.^6
e?-9V ฃC~

Temperature
Wet test
Meter
tw,
ฐF
^^
fjซซ
"^o-^
ffJ&&
fJ^^

Dry gas
Inlet
^i*
ฐF
7^,
?*L
***>,
^^5
?^^
"%

Outlet
^0-
ฐF
707,
7a
73-,-
' '7y
^7V7y
^^
ปK77
meter
Average
td.
ฐF
75.^
77 ^J
7^.5^
Sd/7
5rJ.^^

Time
0,
min
/J.5V
7,95
sr./t
/V. 7V
ti/rs

Average m ^
Y






2Z.
AH@






^OTJ"^
Calculations




Ml
0.5
1.0
2.0
4.0
6.0
8.0


AM

13.6
0.0368
0.0737
0.147
0.294
0.431
0.588
Y
Vw PD (td + "60)

\/ /D j. ^" \ /f x /icnl
Vd^pb + ]2.6] Vw /
. 
-------
     Date
Barometric pressure, Pb =;lljl3n.  Hg
                                                          Box No.

                                                Dry gas meter No.
Ori f ice
manometer
setting,
. All,
in. H20
0.5
1.0
*jr
4-0
6.0
8.0
Gas volume
wot test
meter
Vw.
ft3
5
5
•*}$'
10
10
10
das volume
dry gas
meter
V
ft3
. Lffti, O^t~J
tiz.03?

QI s-.uia
OiJ-.fe'i'J


Temperature
Wet test
Meter
twt
ฐF
"*V
6> -
''""<• V,
•"•"si
5S ,,
-1 ss


Dry gas
Inlet
tdi-
ฐF
f/
8*K
*^
f<"h,
1M-v,


Outlet
'do-
ฐF
^•y
-ป*„
7C-"-,,
J3^,V
?%S,S


meter
Average
td.
ฐF
7%
-------
     Date
     Barometric pressure, PJ, =JgvT, r", oo
J3ฃ-. VoV
O.? 5=. -7TP
.'i'V. 7 J~J,
,VT/. JO-/

Temperature
Wet test
Meter
twป
ฐF
IV? -j .
/y 7c^
/07<5
^^^
^'V'/
>0-^f

Dry gas meter
Inlet
ldi.
ฐF
!JJ
^*
^^. .
7"
'~*,rt
oa
'v •".,ซ•
^a>
"*• 111

Outlet
tdo*
ฐF
'^77
"fiV;-..
"^V*
'-
-------
     Date
     Barometric pressure, Pj, ^VC-n. Hg
          Box No..

Dry gas meter No.
Orifice
manometer
setting,
AH.
in. HjO
0.5
1.0
/,ST
ซ3.o
J-o
8.0
Gas volume
wet test
meter
Vw.
ft3
5
5
10
10
10
10
Gas volume
dry gas
meter
V-
ft3
^07. io&
<••• i tii f)~t*
^/j.o^y
e/S.rt^*'/
v-*X V /"If* f?
ซ?Ci. o-c 7
C7-J..J ? 1 C
h?-?-?. 5 /ซ?•
r-t ••.•..•.."-',-.

Temperature
Wet test
Meter
^Wt
ฐF
C^^r
"-7.-,?
*v-rCT
0>4; ^.-,
efc.,,
^.v
'Ho
'tfir'
"ซ.V

Outlet
tdo-
ฐF
rซ -,
^7
fc*7/ซ
7y^,c
"p^r<
tf6~?
meter
Average
td.
ฐF
7x.r?
l?ijfj
^-f ^ j
77/7
/M.50

Time
0,
min
6.?

AllL3
0.0317 All f(tw * 460) el 2

Pb (fcd + 460) L Vw J
/, 7 ฃ7 A
/,
-------
                    OMAUMTMHMm  SHEET.
                                                      OF.
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-------
BY
CHKD BY.

PROJECT.


SUBJECT.
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                                       Rffettler
                                      INSTRUMENT CCfiP3!<*TlCN
                                     ItCMMICIAN
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:.'.: .•::, . : . -r- v-V ."V -.-.* •':."
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• ^. .*:!- - ;:. -. "*" .. "
."'••' ^ . •••-."...

• • a • •• , 4 fj A
H SERIES ANALYTICAL BALANCES • . [
-'-••- - *' Jtf •'•- "' • '.•* •
' . * "v :"'• f.'.icit) Semi Micro "?

... •!•;" ..„!'! ^|K, '••'•'.'. H51 . ?4 H51AH
.'."-•• •'••" /*.'•:•'"; ::-^ •' '•"• • '••' Ci' > *••? r^-?-"""* •
' SPECIAL'FEATUR'ES '.•.v-'W/h.'?' :-''-~>: ~" '•••'• - -optical tare v;iJ~ release .
' WEIGHING RANGE-". .. j---:A-:V vj; 0-20g-. . 0-160fl.vj;.j>l .0-160 g -
;' Capacity .'•'-•,>:.•;':.•"- r"-.~,^' 20g ..." ' 1 60.1 g -C.vVf.--li 160.1 g
READ ABILITY •'•-..'• ,. .••': . .-•••-,. 0.001 mg • 0.01 mg -:'!:- :,>. 0.01 mg
, Precision (standard (Jeviation) • ..-•; =0.001 mg =0.01 mg— .'.:ซ =0.01 mg
Optical scale range .• - '• ' . -0.5 to -r- 20.0 mg -5 to tl25 mg. -5to-rl25
1 scale div. - -• "-. '. •". 0.1 mg .1 mg '.-::•;-; •_•'ฃ 1 mg
Dijilal micrometer. : n div. = ' ' 0.005 mg :0.01 mg ,".>:;..V 0.01 mg
'Taring- . .-••-•-..; -'•':.••"'..-:. -;?-.?i3 •
By seninj optical scale to zero' • :.' — ' . 0.1 g _>-..r"-;-;.i* 0-1 9 '
• By use of built-in weight-set ." I9.99g" 1S9.9g* /-Vv I59.9g'
.. Buin-in weights .>• ./.'•' -.. 19.99 g . 159.9 g v'-.v-- ..r 159.9 g
Accuracy .:--: . •-- •"•.- \J ฑ0.02 mg . ฑ0.1 mg ."•'!- ~i =0.1 mg
••' "1 (SaSrg step'" •""'".•• .:•.••'. 0.01 g '0.1 g i r.i .'-.-j.. 0.1 g
' Balance housinj— Base . • " ••. " tSV> x 15H in. .Sn x 20 m.-.-::.^ SM x 20 in.
"'.-•.:-.. Height •':-•• ••'-. HBVi in. • ••16inf;>*-'r:'-'TA. 16""- •
Weighing chamber— Base • ..,.-.- :/J 9x6 in.— MS _6*\8hiฃ$ฃฃ 6%xBnu
•" "-.""-•i:~'s..-.i Height V':_^"-",ji MSS-'A: access port : BTn..^.^^^ .8 in.. .'/;
' :' •."^''l~'-Af-";-.-V.--iJ?.r-r/'--ra cBameler = 2ft in. Kr^v-^V-lfi;^.--'''.'-^-.
'•.•-;"''.".Z;i.iv'^7'i'C--z.:..'r-i"V.'-;i height — 114 in. • f-'i*?'.fe3?5jics^3-*.:-"-v-r-"
". Weighing pan— Oiimetsr -"•-.. *••ฃ MS: 1% in. '3%Tn-':i5iv-^ 3V4 in, ..
rtl- ••-:•„•:-•. Pan-bow height :•" i' M5S/A: 1V4 in. '• '/iB'.^Jis^'Si ?.'"-,-
Vr---'v'v:i •• ^;"-:?-'--:— --"vrf M5:4V4in. •-'••- ^^ ci^Wil'^- *-J-
: ":;.r" "•'",-•' -.'''^ •:-<•"'•'••"; M5S/A:3%in. •' *.-•?;>-. Nv^-* ••••-•'=
--wersuppry . ' ' W - 4 110-220 V . -1 10-220 V :..-;-•;. "ฐ-22ฐv
••;-.- -•-.....:-...-'-:-. so-eoHz ' so-ec ป•:••••• ?:i ซ-ซ>* _
Ne1ป-e.^tl •-.- •••.-. 	 ..: 29 to 24ft. -"-.;•• .
Pices EllKtwMjrchl.1976 : 5050./5445. 1850: :" "-%:?. 192S-
•
.: -•• --
O
1 r"
:
iiiQ N77"
i j
""'•'-'•
~,x •' :
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';_ -full range .-
{•"'J'preweigb • • -
j/"J'releass '•• .:
-_ซIull range '
*~~\ari"-i- ; ' ••
>'.-'r>l50g".^.:
; 'I70g ":"!w.'! '•>•
- 0.1 'mg
=0.05 mg .-
; Oto 1000 mg
" 10 mg
. 0.1 mg : •
" 159 gt-'-" '
: 1ฃ9fl..:.'-... -
;..=0.18mg'
ฃi^S^:
'r."zฃ:&&3ฃ;'$
r^'.-^-Z^*-*-'
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!~ -•-.-? TV-- r.; :'••-
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110-220V- '.'
50-60 Hz
. 26 tt> ; • "
1995. .. •
"- • • Jt
• — • • '
j ; .0



*
,.. .,...
% Economy

s"
f H8
|. ••;...•.-;.
\ .vernier
_ ' readout
* "0-160 g '•-•
T! 160 g
": 0.5 mg
= 0.3 mg
". -50 to 1250 mj
10 mg
159 g
v 159 g .
i .ฑ1 mg
^ 9V4x18in. '
- 16 in. - •••
^ 6% x 8 in. ; •
H " • • • * "" "
ป^Vr-~"-- ^.-:;
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. 110-220 V
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• 24 a> •
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'. ^ H72 . '. /ฃ H78AH
:. . -.-..'': '/•''•. rele'ase
• full range" .* • full range
'preweigh- " ;.i preweigh
~0-l60g' -". "i 0-1 60 g
160 g .;• "•> 160 g
0.1 mg ~ ? 0.1 mg
=0.05 mg "• ฑ0.05 mg
) 0 to 1030 mg ; 0 to 1000 mg
10 mg . ': 10 mg
0.1 mg •_• 0.1 mg
159 g' • •• '4 159 g
: 159 g . . •; 159 g •
• =0.25 mg " 4 ฑ0.25 mg
'•lg . •:.-'•:ซ lg
f 9% x 18 in. v? SV4 x 20 in.
" -16 in. : -''.i 16 in.
f . 6% x 8 in.-. -'-;4 6% x 8 in.
;'B 'ai.:; -J:. ^ :^ 8 in. .
' 31i in.;.' i '•'^^ • 3% in.
110-220 V •••••'i 110-220 V
50-60 Hz.'' V'5 50-60 Hz
24 tt> '"..- ft 2416.
'1095.'':' ---'-3 1195.
'WiSioul separate tare fndicatjon
      ' readout bejins at zero rejartless at ta/e used
I

-------
     APPENDIX E




PROJECT PARTICIPANTS

-------
The following Weston employees participated in this project:
Peter J. Marks
Department Manager
Laboratory Services

Barry L. Jackson
Supervisor Air Testing

Jeffrey D. O'Neill
Assistant Project Scientist

Gregory L. CeJ iano
Assistant Project Scientist

Charles Dobroski
Laboratory Technician

Theodore B. Moxon
Laboratory Technician

Richard J. Urban
Laboratory Technician

John Wi11iams
Laboratory Technician

David N. Maloney
Laboratory Technician
econENVIRONomics Division
econENVIRONomics Division
econENVIRONomics Division
econENVtRONomics Division
econENVIRONomics Division
econENVIRONomics Division
econENVIRONomics Division
econENVIRONomics Division
econENVIRONomics Division
Others:

Dennis P. Holzschuh
Technical Manager
Emission Measurement Branch
Environmental Protection Agency

-------
  APPENDIX F




OPERATIONS LOG

-------
            No.
               IMP MILL DAILY OPERATION REPORT
  RED GRADE
    D -
                          PRODUCT GRADE
  CLAYFROM
                          PRODUCT TO
                        ^a.
  TIME
% MOIST.
PRODUCT TO
STARTED
STOPPED
  10
  11
i 12
  AVE.
                                                         OPR. TIME
                                                         OPR. —-'.
                                        i> o
  10
  AVE.
                                                         OPR. TIME
                                                      /
                                                         OPR:';'-- '-'-"-/ '
  11
  12
  AVE.
                                                        OPR. TIME

-------
           No.
                IMP MILL DAILY OPERATION REPORT
RED GRADE
                                                  Dotซ  --.
                                                         /.  *;?
                            PRODUCT GRADE
CLAY FROM
'.'T-'- 'X  /'.'../ ^?1 .*ป,-.-
            PRODUCT TO
TIME
% MOIST.
PRODUCT TO
STARTED
STOPPED
SPEED
10
n
12
 AVE.
                                                          OPR. TIME

                                                          OPR.
10
 AVE.
                                                          OPR. TIME
                                                      tfT
11
                             H'o*
12
AVE.
                                                         OPR. TIME
                                                         OfR.
                            A CLEANER PLACE IS A SAFER PLACE ^ |f

-------
-.. I
'JNo.
                    ROLLER MILL DAILY OPERATION REPORT
                                                                    s^w-

TIME
7
8
9
10
11
12
1
2
FEED- GRADE * ^ PRODUCT GRADE ? , ^/ > ^
GRIT
t f o
•JO 6 t

''IL'':' '
•fc&ซ
ซf*.V
/ปป<*•&
ป v*.**.
AVE.
MOIST
-r'1
/•• *
• ' .'

.!.' **
' '•*

J * ^
; '••
iREEVES^
!^^S:'
• - * . .- ' '•


• • i
'::*f"\-;;: *



PRODUCT TO
5^1 ^l^o
' • ' t

'•. •' ; :', ':' ฐ ••-•''-'


. ซ ,

TIME
.STARTED
.y,>-ป ;
."•• •"•' •-•'•• '
n
:• ^ •
••,-,- . , .''..•''.;'" '. "

'•-.-"" " . • " ' *
^%3V
STOPPED
5*1*0 O


, ' '•' ."--••
3;*"ซ, •&.:...
"-','.-: ' ,


REMARKS
Ift^JSC, ^ v
^k H5 H
A 0 ฃ ?t*t
'.••• ..' ' '
• ' •"'•'. •''•' • - ','•
:•'••'• . ,.•:'< - :

/
•-:-. . v -\ ;-".-•• ....... :. . '-., /'•••;..•'•' "•''''••'••''•': S '-
        /*,  i r r  '
       I ^M> N>
                            TONS/HR.
                                           TONS PRODUCT
OPERATOR
10
AVE.
OPR. TIME
                             TONS/HR.  ?'
                                           TONS PRODUCT
                          \
OPERATOR
                                          M
12
AVE.'
OPR, TIME
^. A\'i- - "^
                    TONS / HR.
                                                   TONS PRODUCT
OPERATOR
TOTAL OPR. TIME
                    TONS / HR.
                                                   TONS PRODUCT

-------
     NO.
                       ROLLER MILL DAILY OPERATION REPORT
          FEED GRADE
                                          PRODUCT GRADE
TIME
 GRIT
               MOIST
REEVES
PRODUCT TO
                                                       TIME
                                             STAR
                                                           STOPPED
                                                               REMARKS
                                                           3> f
          8
   o
  11
  12
$3
  AVE.
  OPR. TIME
                        TONS/MR.
                                                      TONS PRODUCT
  OPERATOR
                                                                      ;; -ft  '
                                                                      J&f.f.lJ*
       >  *>-/>
  10
  AVE.
  OPR. TIME
                  .-3L
                              TONS/HR.
                                                TONS PRODUCT
  OPERATOR*
                .-> ^
  11
                                      f/.^o
  12
  AVE.'
OPR. TIME
                                TONS/HR.
                                                TONS PRODUCT
  OPERATOR
  TOTAL OPR. TIME
                        TONS
                                                      TONS PRODUCT

-------
          NO.
ROLLER MILL DAILY OPERATION REPORT
                                                                        J

TIME
-•" '7'"' '
'••• '8 :
9
. 10
11
-'*ป''
, '..' 1 '
•'•',' 2 "
FEED GRADE - * - PRODUCT GRADE > g# f -+ T^ A
GRIT





*"
r
i

AVE.
MOIST


i •
'


>
•

REEVES



^
.s
t.
V.
"
,r
PRODUCT TO
'

* '
•V
* •• -
t *•
* ^
: 'v
TIME
STARiti)


•
t ;



^ •
STOPPED
:

V
'1
It
^
j
• ~ . *•

'
REMARKS

*
-
*


•*
i
4
                                                                                   jk  .
OPR. TIME
         TONS/HR.
                                                       TONS PRODUCT
OPERATOR
          /)
                             n
    •;*,
10
AVE.
OPR. TIME
OPERATOR
                               TONS/HR.
                                  TONS PRODUCT
11
   o o
                                              **>
12
 6
AVE. "
OPR. TIME
         TONS AHR.
                                                       TONS PRODUCT
OPERATOR
TOTAL OPR. TIME
         TON8/HR.
                                                       TONS PRODUCT

-------
NO.
ROLLER MILLPAILY OPERATION REPORT
      '  V  -f''   '   -' '• •'•'  -  •*•**•*+
 • •••:•    ••  -^  •   .  •  •   -   Date. '' s*-   -*  **


TIME
'l
9
9
10
11
12
1
2
FEED GRADE PRODUCT GRADE (-. '— '^f*"". •
GRIT
^ 76
/CftCx
ll&
*")• Vi "^
r^iv
S-?9.-"
/^•^ T>t>
I^^^Q
AVE.
MOIST
\**1
1^
t ป ^.
V* fe
/ป!l
V^;;
S; ^
^.. ^

REEVES
^'^"0 .

iU

• •'_'.-.' . '; '




• OPR. TIME ฃ5- V\ CV*
PRODUCT TO
S/i"i2/^o

'.--/ ' •

• ' •*• ' • Ji '''.''''•' ~ * '
• ':. •;• .-. ' -.- .. -•.• .'

.

' .;' ••"• ;.;"" '
• -• • •"-' ..'•'' - .'

^:sv
STOPPED
2C ^ •
• • - .

'. . • • • '.
•'• •'•'^•'•':.
'. '.•":/:/ ••'-'•'•' '•'•


REMARKS
• ' -
1- 1
6r\ 6' It
t f>r^
: .•,...•.,'
-•'••- .' ' ' ',


. ' ' • '•••'.''" ;•''•'•.'' ' .. • • - ••,-'! . • •
TONS/HR. TONS PRODUCT
•WLt^rt ' •'•''''• '" • '" • ''•' • : '
OPERATOR •-•••
3
4
5
6
7
8
9
10








AVE.

• j . ''..:- -•
• . . ',,



•
?>#$








%jT&

OPR. TIME / fr?L
ff$i-bi
J~ & ~ ฅ$





^"ฃ3-1?



' ' " •'•"'. ,-
- '' ' • -- .#• 'ฃ'•
;>'*)','

•; 30


• '. - 1




//;^^




' . •/'


•
TONS / HR. TONS PRODUCT '
' ' "*" ' :
---s .•'•'.." ••••••• •'••• • . - •• . • •
, S . , • • • : ...
OPERATOR _x} ]}**&,•ฃ„>*" . . ' .-•••..'
11 S
12 S
1
2
3
4
6
6 ป
)" H d
' ^,,<





7Po
AVE.
& c%
'•'*•• / ^





%*c&
ซ-
s! ฃ &**'.




• • .

*>) S**v i
• •* ^ u T

OPR, TIME^Pi^^ „•"..ซ•'' '^
i-i-  ^ ••-.^••JP<'.'"J* " ' • ' '• ' •'•'•"
TOTAL OPR. TIME . TONS/HR. TONS PRODUCT

-------
       SUPGRADJ
                  DRYER m\X OPERATIOOEPOBI
                 '                    DATE  /** ' ป  *
                    •sir
       TIME
               Slip
Flit.
                             CfltfX
                                  Vac.
                                       RPM
                                            Molit
                           Drop
                                                       Hr.
                                                     ST
                                                    From
                                                              Grad
                                                                For
Tons
Lost
Rcfflarici and' Explanation
     of Delays
       7A.M.
       8:00 •
       9:00
       tftOO
       11:00
       12:00
       1:00
   <    2:00
                                  •:**X*
       AVG.
                      .     •
        Oryw Operating Noun:  /
                                                                  Total Torn Fed:
Filter Hour*:
A_	   C_

ft          '  D_

Total.
                               Avg
           /T/niK HF .  ~  9, }
                                                           Explanation of Dซgradthg and/or Loueir
                                                                  Gas  Meter at Start -
                                            3o/B     ^
       3P.M.
       4:00
       5:00
       4:00
       '7:00
       8-.00
       7:00
       10:00
       AVG.
                               Dryer Operating Houn
                            V
                         : "vj
                                                                  Toปol Tons Fซ*
                                                                       *X   T •
       Filter Mount
       A          C
       1:00
        Av8. T/FIIti Hr.
                                                           Explanation of Degrading ana/or Loiiej:
       2:00
       3:00
       ioo '
                                                    f
                                                   ^,
       6tOO
                                               -55
       AVG.
                               Dryer Operating Houni
                                                                  Totol Tore Fed
                                                                              /IT~ 'O
Filter Houru
A


*'___•

Totol.
                                        . Hr.
                                           Explanation of Oenrodinq ana/or LOMM:
                               Preuei Fed
                               Operator
                                                                  Gas Meter at Start -
^^^IK^SS^riMSI^I^^

-------
      SUP GHADE
                                  DRYER DAILY OPERATIOH REPORT
TIME

7A.M.
8:00.
9iOO
10-.00
tlKป
12-.00
IiOO
' 2:00'
"AVG.
SP. jff.
Slip





'9W



Flit.





jw-C



. Filter Hour*
• .A •= • "o< -
'• V' '•' ' .•' o "•.„•-
Total


3 P.M.
4:00
5:00
6:00
7:00
8:00
9:00
. 10:00
AVG.

••






••






_ ^ *

*
Filter Houns
A. - ' - .C ' •"
' B "• '
':.b ' •
Total . '

11 P.M.
12:00
1:00
2:00
3:00
', 4M) ?
5:00
4:00'
'•AVG.
_ ;










' i . •





'•.
Filter Hour.: ..
- - A ' - C ' ' ••
ป ' ' D . '
Total*
Temp.





•*>' '',

>•
Voe.





^j •


KPM





V V*'

,"l
-Prod.
Moist
^y,
/
PW

;?*
A
;-, /•
'V-
j
5Mln
Drop
ซ-•
4-
s


v.
, v>..

TonV
Hr.
?*;
7'if

?t
t*
r~

Feed
From
^Jl^Q
1'

:ป••'
^


• ' . '^. '. /• '
Dryer Operattno Houn: to
Avg. T/Fllt. Hr 7 - iT- -•
'pnmoFed •ป''•'•'"'•" - • '' •'
Operator V*'
oS




t





./



;•.


'' ป• :



/_
•^
.'•'


3$

&%

?<&

ป6fi










^
fa,

fa
,'
f.6

U
;•'..
y •
&+#
^
*^r

x".-

x

Dryer Operating. Hours: cf •
AVQ-: T/Mlt. Hr. '
Prena Fed Jf.
' ' - - - /'^ '•"••' '
Operato7~>ty>E>-ป -xt ~&*&-&-v~*~^.
* fj ^.






1


•) •








•V- '
•.•'"' J
^ •



i&x
' r
Crtf*>
I'?,*
'X^"'
Ifo^f
f
ป• f*.
fa*
.. _*
g;.-

8'v

'/
•>

,t-

fc

ffa

^c

ro

i5W

,ปrป.

• i

i ,

• . • .•-. . .•• ;.-• •• .:-. ^.<7':.. . •;•;.•
' Dryer Operating Koun: '•'' ',' '
Avoซ T/F!lt. Hr. ', ' ' Q, &
Prenei Fed [/ // :
Operate^ >jyv "SfaffiTZT
Prod.
To^
Si

/• .

ปป



Grade
For
Tfjti
^K
M
-i
ft-
fy
-&

Toni
Lost
f- •





'
r4T.
Remorki and Explanation
of Delayi

. . ป

• ' .
: - ' ' '

• ••'"'. •• '-''-' '•" s .
' \ • " " ' ' "
Total Tonป Fed: ' $*.f^ j2>
• Explanation of Degrading ana/or LoiMt:

Gas Meter at Start - ;











* "'


.- • '
/ '.• -,; • • •'•'•'• •
/ lฃ t)
Total Tonป Fed **< X^ ' .',••. . •
.< ••
' Explanation af Degrading and/or Louซt: •
. ' , ' •••' ' • ' ' . ' .•
Gas Meter at Start -
• I

            ^^^^                                                           'v(- •:.•'ซ*••

-------
 /.       We
                   -7,7
         P.O.  |(o
           H P     HY&
                              64 T3ป/
10
                     A /
*.
                Z. -  J-L.
                    C Y=M
         4 .S^
          -
          -  a O O    C
                      c.

-------