EMB Reoort No. 78rOCM-12A
November 1980
R POLLUT
EMISSION TEST
CD
O
LH
SOCMI - Fugitive Emissions
Ethylene Production
Union Carbide Corporation
Torrance, California
November 1980
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Office of Air and Waste Management
Office of Air Quality Planning and Standards
Emission Measurement Branch
Research Triangle Park. North Carolina
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EMB Report No. 78-OCM-12A
Emission Test Report
SOCMI
Fugitive Emissions
Ethylene Production
Union Carbide Corporation
Torrance, California
November 1980
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I. Introduction
Under the Clean Air Act, as amended, the Environmental Protection
Agency is required to develop standards of performance for new stationary
sources. These standards are based on the best systems of emission reduction
(considering costs) that have been demonstrated. EPA is currently developing
a standard for fugitive emissions from synthetic organic chemical manufacturing
processes, and testing was performed at this facility to gather data for
this study.
Testing was performed at Union Carbide Corporation's ethylene unit at
Torrance, California during October 13-19, 1978. Emission Standards and Engineering
Division, EPA and Engineering Science, Inc., Arcadia, California, personnel
performed the testing.
The purpose of the field study was to perform a complete individual equipment
survey with a portable VOC analyzer to measure the local VOC concentration
around the item's potential leak source, and based on that data, compute the
frequency of occurrence of leaks based on different concentration-limit criteria.
A second purpose was to compare the effectiveness of an area monitoring system
in this unit for indicating the presence of leaks when an overall equipment survey
is used as a base for comparison. Unit walkthrough surveys with a portable
analyzer were also conducted for comparison of leak detection effectiveness.
Finally, vapor and liquid samples were collected from selected sources
for chromatographic analysis to compare vapor-liquid distributions of individual
organic compounds.
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II. Summary of Results
The results of individual component surveys are presented in Table II-l.
The frequency of occurrence of VOC readings in various ranges are presented
for each general equipment type and for all equipment screened. The results
of the walkthrough surveys will be analyzed in a separate report. Due to
the relatively high frequency of occurrence of VOC concentrations >10,000 ppmv
for all equipment types and the lack of elevated readings from the fixed point
monitoring, it appears that the fixed monitors in use are ineffective for
identifying these fugitive emission sources. However, the monitors were designed
for personnel "exposure and detecting explosive mixture formations and not
for fugitive emissions'--control.
In one area of the unit, a repeat screening of individual equipment
was conducted. The separation area storage tanks were first tested on
October 16, and were retested three days later. During the repeat test,
different instrument operators and data recorders performed portions of
testing. Also the individual components were not uniquely identified.
Therefore the results presented in Table II-2 represent the combined varia-
^
bilities resulting from method repeatibility (different instrument operators),
item identification (different data recorders) and variations in leak
magnitude. As can be observed in Table II-2, the reproducibility was
good for concentration results less than 200 ppm and greater than 10,000 ppm.
For measurements between these two points, the data were more often different
than they were the same.
The field data sheets are included in Appendix B.
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The results of the chromatographic analysis of vapor and liquid
samples are given in detail in Appendix A. This appendix incorporates
the report prepared by Engineering Science, Inc. for EPA describing the
methods used and complete results. Sample identifications are given in
Table 11-3. For the purposes of this study, the compounds were identified
and grouped by elution times equivalent to normal paraffins. It is expected
that the majority of the compounds "measured were actually unsaturated olefins.
III. Process Description
Union Carbide's Torrance chemical plant thermally cracks purified
refinery gas and distills the product to make ethylene and acetylene. The
ethylene is then used to produce polyethylene. The plant was started up
in 1956 and has been in almost continuous operation since that time. The
plant was operating normally throughout the test period.
IV. Sampling and Analytical Procedures
The instrument used to conduct surveys at this facility was a Century
Systems Corporation OVA-108 organic vapor analyzer. The instrument was
calibrated daily at the test site. Methane in air standards were used.
Unit walkthrough surveys were performed by first identifying a proposed
path so that the unit perimeter would be traversed, and that all pumps and
control valves at ground level would be surveyed within a distance of 1 meter.
The instrument was then carried through the unit along this path with concen-
trations and location notations recorded on a strip chart recorder.
Individual component surveys were performed by traversing at the surface
of the potential leak interface to determine local VOC concentrations. The
highest observed concentration was recorded on a field data sheet.
The procedures used to collect and analyze the vapor and liquid samples
are described in Appendix A.
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Table II-l: Summary - Number of Components Versus VOC
Concentration at 0 Centimeters from the Source; Union Carbide Corporation, Torrance, California
VOC Concentration
ppm as hexane
< 200
201-1000
1001-10000
> 10000
Total
Equipment Type
Pump
Seals
#
30
9
1
11
51
%
59
18
2
21
Control
Valves
#
85
13
5
25
128
%
66
10
4
20
Other
Vatves
#
1554
203
108
436
2301
%
67
9
5
19
Open Ended
Lines
#
287
40
16
•43
386
%
74
10
4
11
#
%
#
%
Compressor
Seals
#
3
10
4
25
42
%
7
24
10
59
Total
Equipment
#
1959
275
134
540
2908
%
67
9
5
19
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Table II-2: Summary of Results
Repeat Screening of Separation Area Storage Tanks
Test A: 10/16/78
Test B: 10/19/78
voc
Concentration
0-200
201-1000
1001-10000
> 10000
Measurements
with same result *
Number
77
6
11
65
%
85
24
44
93
Measurements
with different result
Number
14
19
14
5
%
15
76
56
7
*Test A used as reference for determining VOC range.
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Table II-3: Liquid and Vapor Sample
Identification and Descriptions
Sample Number
577 000 089
090
091
092
093
094
095
096
097
098
099
100
101
102
103
104
105
106
107
Collection Location
Separation Area, Pump
DH 38
Separation Area Tank
Farm
Separation Area Acetone
Storage Tank
Separation Area Crude Drip
Storage Tank
Separation Area 1#
Res. H.E. Liquid Trap
Separation Area Pump
#38
Separator Area Concentrates
column kettle
Separation Area Vent
column bottoms
Separation Area - Vent
column bottoms
Separation Area - Dripolene
still bottoms
Separation Area - C^
column bottoms
Separation Area - C3
column
Separation Area - Ethylene
product pump
Separation Area - 0# propane
subcooler on primary pump
Cooling Tower Water Inlet
Cooling Tower Water Outlet
Glycol/Water Cooler
Liquid Concentrates Vaporizer
Sample Type
Vapor leak from
pump seal
Ambient vapor
sample
Vapor - Leak from
valve
Vapor - Leak from
valve
Vapor - Leak from
valve
liquid from trap
Vapor - Leak from
pump seal
Vapor leak from
open-ended line
Vapor leak from
control valve
Liquid from.
control valve loop
Liquid
Liquid
Vapor leak from
gauge valve
Vapor leak from
valve
Vapor leak from
valve
Liquid
Liquid
Vapor
Vapor leak from
control valve
-------
Table II-3, Continued
Sample Number
108
109
110
111
112
113
114
115
116
117
Collection Location
Furnace Area Clarifier
Furnace Area Clarifier
feed liquid
Furnace Area Clarifier
overflow effluent
Separator Area Storage
water seal drum on N 2
dripolene storage
Separation Area C2H. Mix
storage tank
Wastewater Treatment Area
Wastewater Treatment Area
Wastewater Separator
Wastewater Separator
feed
Sample Type
Vapor over clarifier
Liquid
Liquid
Vapor over drum
Liquid in drum
Vapor ^ Leak from
drain valve
Vapor - Leak from
covered manway
Carbon cannister vent
Liquid - water discharge
Liquid
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APPENDIX A
LABORATORY REPORT
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VOC EMISSIONS FROM A
POLYETHYLENE MANUFACTURING PLANT
Contract 68-02-2815
Work Assignment 28
Submitted to:
U. S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Research Triangle Park, North Carolina
Submitted by:
Engineering-Science
7903 Westpark Drive
McLean, Virginia
April 1979
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DRAFT
TABLE .OF CONTENTS
Page
SECTION I INTRODUCTION 1-1
SECTION II SUMMARY OF RESULTS II-l
SECTION III ANALYTICAL PROCEDURES III-l
Field Testing III-l
Laboratory Analysis of Liquid
and Head Space Samples II1-2
APPENDIX A RETENTION TIME DATA
APPENDIX B STANDARDIZATION RESULTS
APPENDIX C CALCULATIONS AND DATA WORKSHEETS
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DRAFT
SECTION I
INTRODUCTION
The United States Environmental Protection Agency, Office of Air Quality
Planning and Standards (OAQPS) is currently investigating the magnitude and
nature of fugitive volatile organic carbon (VOC) emissions from petrochemical
plants for the purpose of recommending appropriate emission standards for that
industry. Engineering-Science was issued Task Order Number 22 under Contract
Number 68-02-2815 to provide field testing capabilities for development of
fugitive emission data from a petroleum refinery.
The field test program was conducted at the Union Carbide Corporation's
Torrance, California polyethylene facility during the period from October 19,
1978. The test program utilized two portable total hydrocarbon analyzers
(Century Organic Vapor Analyzer, OVA) and a TRACOR Model 550 gas chromatograph
(gc) equipped with dual flame ionization detectors. This report presents only
test results obtained with the gc.
The remainder of this report is divided into two sections as follows:
Section II - Summary of Results
Section III - Analytical Procedures
In addition, example calculations, and laboratory data are presented as
appendices.
J-1
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DRAFT
SECTION II
SUMMARY OF RESULTS
The results of the analyses of the syringe samples collected and ana-
lyzed during the field test program are presented in Tables II-l and II-2.
Table II-l presents the results in terms of specific concentrations in parts
per million by volume (ppmv). The values presented in the table are in terms
of actual ppmv of each compound* The total ppmv for each sample is presented
in terms of methane. Table I1-2 presents the same results in terms of weight
percent distribution of the various hydrocarbon groups. The total weight per-
cent of. reactive hydrocarbons (all non-methane and non-ethane hydrocarbons)
is presented at the bottom of Table II-2.
Table II-3 presents the results of the laboratory analyses of liquid
samples collected during the field test program. The values presented in
Table II-3 are weight percent of each hydrocarbon fraction. Total hydro-
carbon concentrations in parts per million by weight and the percent total
reactive hydrocarbons (all non-methane and non-ethane hydrocarbons) are pre-
sented at the bottom of Table II-3. Table II-4 presents the results of
head space analyses of a few liquid samples. Reproducibility of the head
space sample analysis was extremely poor and attempts to continue the
analyses were abandoned.
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DRAFT
IA3LE II-.
VDC ANALYTICAL SIWIARY
VOC Concentrations
UNION CARBIDE - TORRANCE, CA. - FIELD SAMPLES
089
090 091
092
093
095
096
097
PARAFIRS;,
ppm HC
. 2106
5852
23,364
12
11,202
73
C3
60
22
50,474
C5
363
C8
C9
AROMATICS
•OLEFINS
18
238
10,280
26
13,037
95
2,566
133
116
1,558
* As methane.
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DRAFT
ABT2 II-l (Cent.,.
VOC ANALYTICAL SUMMARY
VOC Concentrations
UNION CARBIDE - TORRANCE, CA. - FIELD SAMPLES
* As methane.
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DRAFT
II-I tCont.)
VDC ANALYTICAL SUMMARY
VOC Concentrations
UNION CARBIDE - TORRANCE, CA. - FIELD SAMPLES
114
115
PARAFUiS,
ppm EC
s t "/
20
12
C3
11
C5
C6
C8
Cg
^OLEEINS
C5
C6
19
17
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VOC ANALYTICAL SUMMARY
Weight Percent
DRAFT
TABLE II-2
UNION CARBIDE - TORRANCE, CA. - FIELD SAMPLES
SAMPLE NUMBERS
089
090
091
092
093
095
096
097
PARAFINS
WEIGHT PERCENT
100
88.3
38.6
2.4
82.5
1.1
C3
5.5
1.3
C4
C5
3.0
90.6
C6
C8
Cg
AROMATICS
OLEFINS
37.5
7.2
34.0
10.6
9.3
4.3
12.7
81.5
2.6
C4
10.3
* As methane.
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DRAFT
VOC ANALYTICAL SUMMARY
Weight Percent
TA3LL 11-2
UNION CARBIDE - TORRANCE, CA. - FIELD SAMPLES
*As methane.
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DBAFT.
VOC ANALYTICAL SUMMARY
Weight Percent
UNION CARBIDE - TORRANCE, CA. - FIELD SAMPLES
SAMPLE NUMBERS
114
115
PARAFINS
WEIGHT PERCENT
5.3
24.5
C3
1.6
3.8
11.8
C5
6.7
C8
C9
AROMATICS
OLEFINS
C2
10.2
2.4
70.4
1.3
C6
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DRAFT
VOC ANALYTICAL SUMMARY UNION CARBIDE - TQRRANCE LIQUID SAMPLES
-------
VOC ANALYTICAL SUMMARY UNION CARBIDE - TORRANCE LIQUID SAMPLES
SAMPEE NUMBERS
110
112
116
117
PARAFTNS,-
WEIGHT PERCENT
0.028
0.009
0.178
C3
32.078
14.785
C5
63.614
0.826
15.169
8.344
C6
0.255
0.049
0.041
2.424
1.028
Cg
6.858
0.003
1.360
0.546
19.973
0.041 51.168
44.972
AROMATICS^
TOTAL ppm
2800 8600 560
260
TOTAL REACTIVE
99.972
99.991
100.000
99.822
HYDROCARBONS
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DRAFT,
. .- . -- J. J-~ H '. '_ v. ,. C. . )
VOC ANALYTICAL SUMMARY UNION CARBIDE - TORRANCE HEAD SPACE SAMPLES
098
To]
09«
Bottom
099
104
105
ppm HC
0.019
0.001
1.035
1.290
0.021
C3
0.010
0.439
0.259
C4
0.353
0.001
0.105
1.032
2.321
C5
0.039
6.809
14.413
0.268
3.244
0.106
8.857
1.311
0.904
1.980
2.909
0.379
1.092
C8
7.688
0.312
1.639
32.671
31.450
C9
5.960
1.105
0.045
0.371
34.958
0.906
4.215
61.283
56.356
AROHATICS
OLEF1NS
16.208
0.000
0.487
0.068
C4
0.736
1.453
78.909
0.047
TOTAL ppm
TOTAL REACTIVE
HYDROCARBONS
99.981
99,999
99.979
98.965
98.7J.O
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DRAFT
SECTION III
ANALYTICAL PROCEDURES
FIELD TESTING
ES employed a TRACOR Model 550 dual FID gas chromatograph for deter-
mination of the composition of grab samples provided by the EPA test team*
Samples were collected in glass 100 cubic centimeter syringes. The gc was
equipped with a gas sampling valve and 1 cc sample loops. The valve inlet
was sealed with a septum. Samples were injected from the glass syringes
through the septum and flushed through the gas sample loops. A minimum of
20 cc of sample was used to flush the valve prior to each sample injection.
After duplicate analysis of a single sample or standard, the gas sampling
valve was flushed for several minutes with zero grade air (total hydro-
carbon less than 1'ppm) prior to injection of the next sample. All samples
were analyzed on the same day as their collection. Between the time of
collection and sample analysis, samples were stored in an opaque container
to protect against component degradation.
The column used for the analysis on the first two days of testing
(October 13 and 16) was a 6-foot by 1/8-inch (outside diameter) stainless
steel column packed with 5% SP 1200/1.75% Bentone 34 on 100/120 mesh Supel-
coport. Compounds of primary interest were olefins and aromatic hydrocar-
bons. ES established retention times for approximately 15 compounds inclu-
ding benzene, toluene, xylenes, straight chain paraffins through Cg and
straight chain olefins through Cg. Satisfactory separation of ethylene
from ethane was not attainable using the SP 1200/Bentone column. A 9-foot
by 1/8-inch stainless steel 100/120 mesh Porapak Q column was rush-ordered
and arrived at the job site on October 16. This column was used from
October 17 through the end of the test program. Column temperatures were
varied throughout the test program in an attempt to optimize separation
but minimize analysis time. GC operating conditions are presented in
Appendix A with associated retention times.
Instrument calibration was performed using benzene and propane standards.
Relative response for other compounds was determined by a single standard gas
III-l
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DRAFT
injection since published response factors could not be reliably extended
over the range of gc conditions used unless electronic integration were
available, which it was not. Both benzene and propane standards produced
fairly good linear response. The results of the standard analyses are pre-
sented in Appendix B.
Under most gc operating conditions a single standard was run for
paraffins and olefins and toluene. This was necessary since no electronic
or mechanical integrator was available and data analysis was based on peak
height. The peak height was a function of retention time as well as concen-
tration.
Some of the syringe field samples collected during the test program
contained hydrocarbon concentrations in excess of the instrument range.
These samples were diluted using 100 cc glass syringes with 3-way stainless
steel stop-cocks. This dilution method was checked using a 1023 propane
standard gas and performing a series of two 50% dilutions on that gas.
This analysis was performed on October 18 under 160°C isothermal condi-
tions. The results are presented in Appendix B as the standard analysis
for that date. Propane concentrations prepared from the 1023 ppm gas were
511.5 ppm and 255.7 ppm.
LABORATORY ANALYSIS OF LIQUID AND HEAD SPACE SAMPLES
Process stream and wastewater samples were collected during the field
test program and returned to the ES McLean Laboratory for analysis. Anal-
ysis of these samples was performed using a Hewlett-Packard 5830A, dual FID
gc equipped with a microprocessor and electronic integrator.
Liquid samples collected in the field were transported to the ES lab-
oratory in McLean, Virginia. Samples were then refrigerated until analysis
was performed. Due to instrument linearity checks, liquid sample analyses
were not completed until March 1979. Although samples were sealed, protec-
ted from light, and refrigerated during the four-month interim from the time
of collection, some sample degradation probably did occur.
Prior to analysis, portions of the samples were gravity-filtered through
Whatman Number 1 filter paper to remove particulate material. One microliter
III-2
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DRAFT
aliquot was injected into a 200°C injection port. The column used for liquid
analysis was 10-foot by 1/8-inch stainless steel packed with 20% SP2100/0.1%
Carbowax 1500 on 100/120 mesh Supelcoport. The oven was maintained at 35°C
for 15 minutes then temperature programmed at a rate of 5°C per minute to a
maximum temperature of 165°C. All liquid samples were run in duplicate.
One cc headspace injection was made from samples 098, 099, 104 and 105.
Example calculations are presented in Appendix C. Field and labora-
tory raw data is also presented in Appendix C.
III-3
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APPENDIX A
RETENTION TIME DATA
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October 13, 1978
Oven'Temperature 175 °C
Column: 5% SP 1200/1.75% Bentone 34, 6' x 1/8" SS, 100/120 mesh Supelco-
port
Injection Port Temperature 130°C
Detector Temperature 200°C
Nitrogen Flow 30cc/min.
Hydrogen 35%
Air Flow 6.5 SCFH
Compound
Ethylene
Propylene
Propane
Benzene
Toluene
Xylene
Samples - 089,
(Minutes )
Retention Time
0.53
0.58
0.50
2.12
3.57
4.83
090
Mean Peak
Height per ppm (cm)
2.86
5.83
0.464
0.347
0.137
No. of
Standards N
5
7
2
2
-------
October 16, 1978
Column: 5% SP 1200/1.75% Bentone 34, 6' x 1/8", 100/120 mesh Supelcoport
Oven Temperature 160°C
Compound
Methane
Ethylene
Ethane
Propylene
Propane
Benzene
(Minutes)
Retention Time
0.35
0.53
0.60
1.01
1.10
2.09
Mean Peak
Height per ppm (cm)
2.35
3.44
3.00
2.26
2.08
No. of
Standards N
0
0
0
6
9
Samples - 091, 092
-------
October 17, 1978
Column: 9' x 1/8" Porapak Q, 100/120 mesh
Nitrogen Flow 50cc/min.
Oven Temperature 130°C
Compound
Methane
Ethylene
Ethane
Propylene
Propane
Butene
Butane
Pentene
Pentane
Hexene
Hexane
Benzene
Toluene
Xylene
Samples - 093,
(Minutes )
Retention Time
0.35
0.51
0.59
1.00
1.10
2.40
2.60
6.20
7.30
17.00
19.00
20.80
51.60
79.80
095
Mean Peak
Height per ppm (cm)
3.48
5.10
4.45
3.35
1.84
0.90
0.33
0.25
0.10
No. of
Standards N
1
1
1
1
9
1
1
1
1
1
1
3
1
1
-------
October 17, 1978
Column: Porapak Q 9' x 1/8" SS 100/120 mesh
Oven: 100-200°C @ 7.5cc/min.
Nitrogen: 50cc/min.
Compound
Methane
Ethylene
Ethane
Propylene
Propane
Butene
Butane
Benzene
Toluene
Xylene
Sample - 096
(Minutes)
Retention Time
0.36
0.50
0.72
1.07
1.40
2.50
2.80
8.10
11.40
16.70
Mean Peak
Height per ppm (cm)
2.18
2.82
2.62
2.75
0.65
No. of
Standards N
1
1
1
1
8
1
1
1
-------
October 18, 1978
Column: Porapak Q, 9f x 1/8" SS, 100/120 mesh
Oven Temperature: 160°C
Nitrogen: 50cc/min.
Compound
Methane
Ethylene
Ethane
Propylene
Propane
Butane
Pentane
Hexane
Benzene
Toluene
Xylene
(Minutes )
Retention Time
0.36
0.45
0.48
0.73
0.76
1.30
2.80
4.99
7.60
18.60
43.60
Mean Peak
Height per ppm (cm)
2.50
4.86
3.73
4.48
4.70
3.52
1.94
0.81
0.86
0.64
0.25
No. of
Standards N
1
1
1
9
1
1
1
1
3
Samples - 97, 101, 102, 103, 106, 107 and 108
-------
October 19, 1978
Column: Porapak Q, 9' x i/8" SS, 100/120 mesh
Oven Temperature: 130°C
Nitrogen 50cc/min.
Compound
Methane
Ethylene
Ethane
Propylene
Propane
Butane
Pentane
Hexane
Benzene
Toluene
Xylene
(Minutes )
Retention Time
0.32
0.51
0.59
1.00
1.10
2.60
7.30
19.00
20.80
52.00
80.80
Mean Peak
Height per ppm (cm)
.826
1.600
2.410
2.690
2.820
1.150
0.980
0.430
0.220
0.160
No. of
Standards N
1
1
1
1
5
1
1
1
3
0
Samples - 113, 114 and 115
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APPENDIX B
STANDARDIZATION RESULTS
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October 13 - Benzene Standards
Concentration( ppm)
1.1
1.1
554.0
554.0
554.0
882.0
882.0
882.0
Peak Height
4.8
4.8
2496.0
2608.0
2560.0
4160.0
4192.0
4256.0
Peak Height per ppm
4.36
4.36
4.51
4.71
4.62
4.72
4.75
4.83
-------
October 16 - Benzene Standards
Concetttration(ppm)
4.77
4.77
4.77
4.77
45.00
45.00
100.00
100.00
100.00
Peak Height
10.6
10.4
11.0
10.6
88.0
88.8
197.0
195.0
189.0
Peak Height per ppm
2.22
2.18
2.31
2.22
1.96
1.97
1.97
1.95
1.89
-------
October 17 - Benzene Standards
13(X°C
Concentration(ppm)
4.77
45.00
100.00
October 17 - Propane Standards
100-200°C
Concentration( ppm)
1023.0
1023.0
1022.0
1022.0
511.0
511.0
15.7
15.7
Peak Height
1.6
14.4
34.4
Peak Height
5069.0
5171.0
4608.0
4710.0
2713.0
2637.0
67.2
67.5
Peak Height per ppm
0.34
0.32
0.34
Peak Height per ppm
4.96
5.05
4.51
4.61
5.31
5.16
4.28
4.30
-------
October 18 - Benzene Standards
Concentration(ppm) Peak Height Peak Height per ppm
1.1 0.91 0.83
45.0 38.25 0.85
100.0 90.20 0.90
October 18 - Propane Standards
Concentration(ppm) Peak Height Peak Height per ppm
1023.0 4762 4.65
1023.0 4787 4.68
1023.0 4608 4.50
511.5 2406 4.70
511.5 2381 4.65
255.7 1209 4.73
100.0 448 4.48
-------
October 19 - Propane Standards
130 °C
Concentration(ppm)
2559
2559
2559
1023
1023
24.2 Methane
1000.0 Ethylene
14.6 Ethane
1000.0 Propylene
15.0 Butane
Peak Height
..6451
6298
6502
2790
2713
20.0
1600.0
35.2
2688.0
17.2
Peak Height per ppm
2.52
2.46
2.54
2.73
2.65
0.826
1.600
2.410
2.690
1.150
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APPENDIX C
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(on srist. pipe rack }
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T. BLOC "321
¥
ID CONDUIT
vors; (ft BI. )?l)
o
fir.
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f
underg found wuJutf run
(undtr ml tracks)
by. u, c, c, - :-..
ceo
-*-!• :'•• | | -\ • II I
(on with pipe rack
conductors to be
m conduit
CONDUIT
. pips ro:k) s
«
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I / /T9 v ,., , -
-------
Appendix C - Test Log
10/13/78
10/16/78
10/17/78
10/18/78
10/19/78
1400-1438
1441-1454
1502-1522
1545-1603
0954-1007
1350-1520
0912-0945
0900-1125
1320-1720
1145
1440
Separation plant walkthrough
Storage Walkthrough
Compressor Bldg. Walkthrough
Furnace area Walkthrough
Polyethylene Walkthrough
Separation Area Storage - OVA
vapor and liquid samples?
Sep. Area Walkthrough
Separation Area OVA
Vapor sample and liquid samples
Compressor Bldg OVA
Cooling Tower OVA
Furnace Area OVA
Furnace Area OVA
Bepeat Separator Area Storage OVA
vapor and liquid samples
wastewater separator OVA
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