-------
FildtaM : C:\2700\6C3\HCF3028.ra* OaUt 8/30/89 8:31 AN Pap 1 of 1
Start Tinai 0.00 ain End Tina* 70.00 ain Low Point: 3246 uV High Point: 610825 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 »V Plot Scale: 100 aV
Chxe*atogxa»
ltfl
a 3 HI fcSSM? M3 55fta:«»tSKK 5? i
?5 JCS9 RCX 3&R RR R RR R9 8 J5 { KB BUI S3 II 9
3~ irfmroiaii mwiif'u niiirriiii'ft
ii • hi
"VftfflTSWn f; mi Kiaiii;';; :;:1
ni
^lA.
II 5 o
,i, I
¦M I ^ I-I I I I Hi | I I I H
11.(7
23.3)
35.00
Tilt (ain)
44.(7
58.33
000081
-------
ID
PESTICIDE 0RGANIC5 ANALYSIS DATA SHtET
fcPA SAMPLE NO.
LSI 3
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Codes Case No.:
Matrix: (soil/water) SOIL
Sample wt/val: 30 grams
Level: (low/med) LOW
V. Moisture: not dec. 2.4 dec,
Extraction: (SepF/Cont/Sonc)
6PC Cleanup: J
-alpha-Ch lardane 164 U
-gamma-Chlordane 164 U
-Toxaphene 3279 U
-Aroclor-1016 1639 U
-Aroc lor-1221 1639 U
-Aroclor-1232 1639 U
-Aroc lor-1242 1639 U
-Aroc lor-1248 1639 U
-Aroc lor-1254 3279 U
-Aroc 1 or-1260 327? U
FORM 1 PEST
1 i37 Rev,
OCCCA a.
-------
Sample Name : L513
Sample Number: 9S192
Operator :
Nelson Analytical 2700 Chromatography System Report Header
4:28 PM
Time
Study
8/31/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
6:12 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR03 7.raw
e:\pkd\MCFR037A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\fltott
IVMCre
e: \pkd\F
2 uL
1.0000 uL
, seq
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT4
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
[ata)
Adjuacad taouac Raw Aaouac Paak Area Paak Be MULTIPLIES
UG/ft£ UC/|C£ [uV-sacI [uV] Ad j/Raw
a n r.nnnmt
» CttBMIE
19.«< BBS
H.H BOO
2i n nraonnim
23.67 OBC
(i ai
i.a» naan,a9
T98.H
iitt tl?B97.ii 5006.a>
9,»*
ifc.it a«»7B.aa imui
»¦»
9».89
1 j fcOai *3161.aa
17 1
at.ei aauMiaa imaitt
138.62
327.38 3.88a6 123916.93
11 <9
0.00
a.ta
0.60
8.«i
V/IL
0.69
Xozmi Ar«* - 81S4X26.50
Cene«acsMleo m 460.&516
Report by Tim Rand, Lockheed-ESC
000083
-------
Chromatoqram
FileName : e:\pkdVHCF8037.rau Date: 8/31/89 4:28 PH Page 1 of 1
Start Tine: 0.00 sin End lias: 47.00 Bin low Point: -1721507 UV High Point: 1993660 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 uV
250.000-
208.333-
166.667-
(U
r~ 125.000-
cry
o_>
CtZ
63.333-
o
o
.667-
ae
&
-0.000-
oa ho oa
„ H~> hO CT> . _
3;* 33 ^ ^ :=• ^
•— • «— CNI CM
n^rW/V-ir
I * * I I I
c_> o
I I
I
c >
»
u >
I I
I I II
f3! I I I I l^p I 1^ I Fj
I I I I I I V-1! I
&
r^-
i i-r i i i i i i | i i i i i i i i i | i
i i i i
-------
Sample Nana
Sample Number
Operator
Interface #
AutoSampler
Rack/Vial
Nelson Analytical 2700 Chromatography System Report Header
4:02 PM
L513
9S192
Time
Study
8/31/89
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time ; 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
6:12 PM
Rav Data File :
Result File :
Instrument File:
Process File ;
Sample File :
Sequence File :
Inj. Volume ;
Sample Amount :
e:\pkd\MCFRQ 3 7.raw
e:\pkd\MCFR0 3 7.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e: \pkd1
e:\pkd\MCFRLND.seq
2 UL
1.0000 uL
Area Reject
0.00
~~~~~EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa Cuapooant Adjuatad Aaevnt Haw tmnt ?«ak Ana Fiik Ht MULTIPLIER
tola) Hum UC/|& UC/|CA tuV-»ae| (uV) AdJ/fUv
23.67 08C
300.14
441.39
3.8«a* IZ3916.93
3.63
¦ W'fc
— VK
WC
Total Axaa - mSMl.OO
Total Caaeaatcatioa » 334.4402
Report by Tim Rand, Lockheed-ISC
isssassss
V
000085
-------
Chromatoqram
Filename : e:\pkd\HCFR037.rau Date: S/31/89 4:02 PM Page 1 of 1 7
Start Tine: 0.00 Bin End Has: 47.00 Bin Lou Point: -1721507 uV High Point: 1993660 uV
Vertical Scale Factor: O.OO Plot Offset: 0 MV Plot Scale: 250 oV
OQ K") oa tji
3 S SI 1
250.000
200.333
166.667
125.000
CO
CXL
83.333
-0.000
7.83 15.67 23.50 31.33 39.17
¦P(
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : LSI3
Sample Number: 9S192
Operator :
Time
Study
8/30/89 3:10 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
0
None
0/0
Channel
attached
A/D mV Range s 1000
Data Acquisition
Delay Time
En d T i me
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount
Noise Thresholds
Dilution Factor:
D ivisor :
Time: B/30/99 3:23 AM
0.00 min.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5035.raw
C:\2700\GC5\MCF5035.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A. amp
C:\2700\GC5\MCF54A.seq
2 uL
I.0000 UG/kg
1
1.00
1.0000
Area Reject : 0.00
Area Threshold : 100
Mu11 i p1i er : 0.68
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T erftoer at u.re
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400 -S-"
.2SMM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY II
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 71
**********
EXTERNAL STANDARD REPORT
Ret Time
Cm in 3
Component
Name
Adjusted Amount Peak Area
ug CuV-sec1
Peak Ht
CuV 3
Raw Amount
u.q \L
1 ?
1 o
JV2-
oia
ijmBHC __
UDTPLII C.
0. 04—
—
12!29
0. 0 6
n—TT
w
ucDccnv
• i /
n o
r*Mnn 1
r94-
PIELBEIN
—
-^•24-rS9—
—205¦73
a*
000087
-------
?S. 17
ENDQ3
¦«.&9 23-V9&^35 1361. 01
101 1 'V
1
* L. C 4
r>r>*r
<=¦ L. OA
Merunvv
1 00 l'")l9 'i? 'Ir't
L-
61.77
DBC
2813.81 3.97a6 131955.50
4137.95
J
LjW
t
Total Area = 4020418.23
Total Concentration - 2829.2379
Report by Doherty Bresnahan
000088
-------
FileNut : C:\2700\6C3\MCF3033.rw Oatas 8/30/39 8M1 AH Pa?* 1 oi 1
Start Tiae* 0.00 ain End Tiaas 70.00 ain Low Point: S2SS uV High Points 187885 uV
Vertical Scale Factor: 0.00 Plat Offsets 0 aV Plat Scales 100 aV
Chromatogra*
ltNH
aa-j
««-:
I
| wrg
¦n
at
3.8H
k.w-4
fe is s"? a J* s sm«=R setie ssm r sua
- MS S 8* t BfcEJlRB* *¦*; 55555 a (Hill a 8ft I
Vnnnrunrnr niririmrf • ^
'••Trrrrj
* f j I | | I | 6 la
¦'I 11 *, i ft. i. 11 fi i "i 1.3 i «•¦ 11 "¦ i r . q
11(7 8.33 35.01 H.U
Tii» (ain)
5».a
000089
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : LSI5
Sample Number! 9S192
Operator
Time
Study
8/30/89 9:07 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range s 1000
Data Acquisition Timet
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
In j. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
8/30/89
0.00 m i n.
70.00 min.
1.0 pts/sec
AM
C:\2700\GC5\MCF5035. raw
C:\2700\GC5\MCF5035A.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF34B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Ra.iect : 0.00
Area Threshold : 100
Multiplier : 0.68
Additive Constants 0.00
Bunch Factor: l
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
3p 1 i t F:at io
T smperature
In j ec 11on T smp.
Detector 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
15 F'SI
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 71
Ret Time
Cmin 3
**********
Component
Name
EXTERNAL STANDARD REPORT """""
Adjusted Amount Peak Area Peak Ht Raw Amount
ug CuV-sec3 CuV] ug\L
_A—StHG—...
D 01 tC
21.71 ftLDRIM-
1*2. 12
39.03 G—CHUPANC
il.00 fl-GHLDf\NE
¦3 '1. 5T DDE
0.14
945.38
0.11
0. 10
260. 00'
595«00-
¦*2.-23
63. 17
2. 39 11831. SI
2-15 i)
-5-t
r-04-
—tlH
12.08
1 i Ol
52738.2S
607.12
4042.'
OLI
17.76
I
a
' S>
ooooao
-------
36. 73 ENDRIN '3.16 <1065.58 3151 G1 4i66 ^
"10.50 DDD 9.58 1')927. 28 958.36 14.0
-------
FiltNaat t C:\2700\GC3\flCF3033.raM Dates 8/30/89 9:08 AN Pa*« 1 of 1
Start Tia«s 0.00 ain End Tiati 70.00 ain Low Points S2S3 uV High Points 18788S uV
Vertical Scala Factors 0.00 Plat OHsats 0 aV Plot Scala: 100 aV
Chroaatograi
mm-.
ItJlH
Kj®4
'».«H
3St4
M
ilW-3 !
31
34-Yrr*i
j>s»-3 ' ""
a *s CSV a as 8 sm*=6 sws sssas;* ssj« c. as*
- »- *?j « ss c bkbhab* hp*; ?:s;rs phiibb a saa
sn
JJLi-
7f--Trw
1, il? S, 1 _»
11(7
23.33 35.00
Tii* (aia)
n.a
B.33
000092
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
t£PA SAMPLE NO.
M14A08
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Code: Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 0.4 dec.
Ev.tract ion: (SepF/Cont/Sonc) SONC
GF'C Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:——— SDG No.:
Lab Sample ID: 9S1S4
Lab File ID:
Date Received: 7-23-39
Date Extracted: 7-31-89
Date Analysed: £ "I
Dilution Factor: 10
CONCENTRATION UNITS:
Llfl/k'3
319-84-6 a lpha-BHC 161 U
319-85-7 beta-BHC 161 U
319-86-8 del ta-BHC 161 U
58-89-9 gamma-BHC (Lindane) 161 U
76-44-8 Heptach lor 161 U
309-00-2 Aldrin 161 U
1024-57-3 Heptach lor epoxide 161 U
959-98-8 Endosul -fan I 161 U
60-57-1 Dieldr in 321 U
72-55-9 4, 4'-DDE 321
72-20-8 Endrin 321 U
33213-65-9 —Endosul-fan II 321 U
72-54-8 4, 4' -DDD 321 U
1031-07-8 Endosul-fan sulfate 321 U
50-29-3 4, 4'-DDT 321 U
72-43-5 Methoxychlor 1606 U
53494-70-5 Endrin ketone 321 U
5103-71-9 alpha-Ch lor dan a 161 U
5103-74-2 gamma-Ch lordane 161 U
8001-35-2 Toxaphene 3213 U
12674-11-2 Aroc lor—1016 1606 U
11104-28-2 Aroc lor-1221 1606 U
11141-16-5 Aroc lor-1232 1606 U
53469-21-9 Aroc lor-1242 1606 U
12672-29-6 Aroclor-1248 1606 U
11097-69-1 Aroc lor-1254 3213 U
11096-82-5 Aroc lor-1260 3213 U
FORM 1 PEST 1/37 Rev.
ct 00c'3
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator ;
Interface # :
AutoSampler :
Rack/Vial :
M14A08
9S184
Time
study
8/30/89 2:03
MCFARLAND
PM
2 Channel : 8 A/D §V Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
1:03 FM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e s\pkd\MCFR031.raw
e:\pkd\HCFR031.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: " Varian 3400-1 GC Column ID: 2250/2401
Rat liam Coapanuie Adju»t«d Aaouac Raw Amount Puk Ana Paak Be MULTIPLIES
(alnl Haaa UG/K&. U6fl0» tuV-s.e) [uV] Adj/SUv
% n *tnam.
I.na HBfEWJl
».» 8SB8i —
in it rirnniiTH
Ell—
If»## OPT
23.7* DSC
>>.aa
¦Ji >Q88J>.88 8>!8>.a»
24, HI
jb.i2 /kmt.n muM
H)il>
t.aawfl 88*18.«i
imaa.ja
IBM
5>8i»*
sa.i» >k»3».i)J—mua.M
121.10
181.0*
I.IW IWtli Tt
Ml«< 30280.91
a.*?
mn—v<-
. \ff-
B'i'BT
0.67
. vf~
. :•>
Total Axaa - H06J*««.00
Total ConcanttatLsa •
Report by Tim Rand, Lockheed-ISC
000094
-------
Chromatogram
FIleNane : e:\pkd\MCFR031.rau Date: 8/30/89 2:03 PH Page 1 of 1
Start Tim: 0.00 mln End Time: 47.00 aln low Point: -1908977 uV High Point: 1214870 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 HV
CL>
cr>
cr»
cm
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
3 c-4 ^9 3 K a! 3 >—5 ^
f«-j ? ? s> p s s s
—1 vH r— crJ 3
CN r«"j •--»
&
2 - g
& S s
I I I
s
I i i in I i3? i I f3! I I I f-f~T Pi T
i i i i i i i i
7.83
15.67
23.50
Time (min)
rl I l i I | I I I I I l I I I j l I
31.33 39.17
I I I I I
-------
Sample Name : M14A08
Sample Number: 9S184
Operator :
Nelson Analytical 2700 Chromatography System Report Header
2:43 PM
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
1:03 PM
Raw Data File :
Result File
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR0 31.raw
e:\pkd\MCFR0 31A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
0.00
***** external standard report*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tim*
Cooponant
Adjuatad Amount Slav Amount ?aak Araa Paak He MULTIPLIER.
Bta)
Nana
UC/|t£,
[uV-iae)
(uV)
Adj/Raw
- t/*-
23.7*
DBC
144.
.92
216.31
2.41.6
50290.91
0
.67
Total Araa - 11333606.00
Total Ceaeaaeracloa » 487.3330
Report by Tim Rand, Lockheed-ESC
0000U6
-------
_ Chromatogram
HleNaae : e:\pfcd\HCFR031.ra« Date: 8/30/89 2:43 PN Page 1 of 1 ^
Start lime: 0.00 "In End Times 47.00 Bin Lou Point: -1908977 uV High Point: 1214870 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nN Plot Scale: 250 MV
gj to lt> r-^ gj in ^ pj
CN -P S K oi IT) id
IC 3»
J*
_ _ . co erj ¦=> en
r —' wJ r—" er» iq
o_>
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000
if
¥ ^
¦ ¦ * CD
i i
v ^ H e
fr . . ¦ ~
a
i i r~i t*i i i i pT i i^r » it i r~j i i i i i i y-1! i | i i*t i i i i i i | i i i i i
7.83 15.67 23.50 31.33
Time (min)
I | i I I I I I I I 1
39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M14A08
Sample Number! 9S184
Operator :
Time
Studv
9/30/89 7:51
MCFARLAND
AM
Inter-face #
AutaSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Ranqe : 1000
Data Acquisition Times 8/29/39 7:57 PM
Delay Tima : 0.00 min.
End Time s 70.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5029.raw
C!\2700\GC5\MCF5029.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF34A.seq
Ini. Volume
Samp 1e Amoun t
2 uL
1.0000 UG/kg
Area Reject
0. 00
Noise Threshold
Dilution Factor
D i v i sor
1
1.00
1.0000
Area Threshold
Mult ip1ier
Additive Constant
100
0. 67
0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400- <3
. 25MM ID .25UMFILM RTX5
30M
HE
20CM/3EC LINEAR VELOCITY
='SI
160
200
300
1 /MIN TO 230
Total Number o-f Peaks Detected: 123
Ret Time
[min]
*********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amoumt Peak Area
ugNJUL t\bL/ CuV-sec3
Peak Ht
CuV3
Raw Amount
up \L
12.39 G-BHC
17.00 HPTCHLK
£Jr, 52--AUBB-I-N
•"» jL UCPCP.ny
~ ¦ VC I IL. I ^ I 'J M
7ft. 14 EN0Q1
83 DIELDRIN
1. 10
1.02
6625»18
5266,. Ql
'). 36 27399. 77
463<33
1 't73. on
1635a 00
-as
'379S7. 7°
iaOfl. 41
oouoaa
^ i
17153. 37
1305.21-
1. 64
Srf
-50
12 i-2-t1
$
c
i
-------
3B.12 EIMD02 S-^6—29565. SO 2182. 11 13. 93 V,
>1.12 ENDALD &*-S9 11663.45 792. 75 12.50
05.98 DDT 54. 46 127754i75 11491. 77 01. 20. ^
36.13 METHQXY 16.'55 7112< 59 599^20 24
61.35 DBC 182.16 261454.11 23415.46 271.88
Total Area = 586418.88
Total Concentration - 308.3305
Report by Doherty Breanahan
000099
-------
FileNut : C:\2700\6C3\flCF5029.ra* DaU« 8/30/89 7:53 AM ?ag» 1 of 1
Start Tint: 0.00 tin End Tim: 70.00 ain Lot* Point: 5268 uV High Point: 63569 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 oV Plot Scale: 100 «V
Chrciatograa
I
¦w
U
5
J n lascs sas«i!3WP;*5i!si?5S«iera jwar saassw
.>1 *k*o» ssiSSiTt ZXKR8»AXRMRM:S;5SS?a RRFXK Fa81S&33
• M ¦ « l« MM Mi I WIMII IHM1I •• Ml lilt I t II I l«M IHMHMKtll IIIIMH lllltl •••*• M IM M» »•«»<• III!
-J I!
3-1'iVrnrr nip
!«a-3 '
* I I
3f I - i - I a 2
!i » j s I ¦ 1 j
ii, i
11.67 23.33 33.00 1l.il 58.33
TiM (mm)
000100
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M14A08
Sample Number: 9S184
Operator :
T ime
Study
3/30/89 8:5:
MCFARLAND
AM
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time* 8/29/89 7:57 PM
Delay Time : 0.00 min.
End Time : 70.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C: \2700\GC5\MCF5029.raw
C:\2700\GC5\MCF5029A.rst
C:\2700\GCS\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
Ini. Volume
Samp Ie Amount
2 uL
1.0000 UG/kg
Area Reject
: 0. 00
Noise Threshold
Dilution Factor
D i v i sor
1
1.00
1.0000
Area Threshold
Mult ip1ier
Additive Constant
100
0.67
0. 00
Bunch Factor: 1
Instrument Conditions
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T emperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400 — S*
.25MM ID .25UMFILM RTXS
30M
HE
20CM/SEC LINEAR VELOCITY
PS I
160
200
300
1/MIN TO 230
Total Number o+ Peaks Detected: 123
**********
EXTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount
F'eak Area
C uV-sec1
Peak Ht
CuV]
Raw Amoun t
uq\L
-BHG-
t1.60 B-BMG
n-RHr.
—».-i+-
38.-90
4. Z(t
952.00
143.21
90970.00-
-406-ItOS-
1 I 'JT
21.52 mLOBIN
20.97 0' 'CHLDANE
-4-r^J
27099.77
r£*A-
30.94 A CI ILDANE-
Q0Q101
-4-2-57-
1 1.29
-6527-1-1-59-
>37213.25
3436.06
^XoTi
¦¦gs. .nja
i-SW>
-oa 09
-44-59-.-75- -
18.77
-46.05
_ ii
-------
¦51.81 DDE —— 151.68 672327.50—578-29-. 47 526.-59- V, -
361 74 CNDHIN- t-3,i<>4 t-7022. 48 1141.94 l'"M"fc6
10.40 DDP i"5"«°09 23Q56. 16 1944.73 2'2.52
<4.55 gMPOSUUgATE Z-.*M 1070^.92-- - -76»l-,4>8 &T-S9-
€i. 1? SMPKgTO 5^4-3 '1916. 19 563.01 \
61.35 DBC 231.42 261434.11 23413.46 343.40
Total Area » 1232967.00
Total Concentration ¦ 490.1710
Report by Doherty Sresnahan
000102
-------
FilefU* : C:\2700\6C3\nCFS029.raH Date: 8/30/89 8:54 AH Pa^e 1 of 1
Start Tin: 0.00 ain End Tiaat 70.00 iin Low Point: 5268 uV High Point: 63569 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Cfcxoiatograa
5 SU9P 8.4 913 3
It RBPnft KaaSBMI
B a tifC* ft*?? S3 SS3t£8KfcZ.=*i=?3Seir:
. » 55555SE IXKMaMRRRR
•II
K
§
U
a
11.67
35.0B
23.33
Ti>* (tin)
000103
-------
ID
PESTICIDE ORGAN ICS ANALYSIS DATA 3Ht£ET
Lab Name! LQCKHEED-ESC Contract: 68-03-3249
t£F'A SAMPLE NO.
M4A06
Lab Codes Case No. »
Matrix: (soil/water) SOIL
Sample wt/voi: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 3.4 dec.
Extraction: (3epF/Cont/Sonc)
GF'C Cleanup: (Y/N) Y pH:
-r*3 NO.
COMPOUND
SAS No. : SDCS No. :
Lab Sample ID: 9S182
Lab File ID:
Date Received: 7-25-89
Date Extracted: 7-31-89
50NC Date Analysed-'
Dilution Factor: 1<
CONCENTRATION UNITS:
HQ/k q Q
319-94-6 alpha-BHC 166 U
319-85-7 beta-BHC 166 U
319-86-8 delta-BHC 166 U
53-89-9 gamma-BHC (Lindane) 166 U
76-44-8 Hep tach 1 or 166 IJ
309-00-2 Aldrin 166 U
1024-57-3 Heptachlor epoxide 166 U
959-98-8 Endosul-fan I 166 U
60—57— l Oi^ldrin 331 J
72-55-9 4.4* -DDE "31 '•_!
"*2-20—8— Endrin _;3i l'
33213-65-9 Endosul fan II T-..1 J
72-54-8 4. 4' —DDD 331 'J
1031-07-3 Endosul+an sulfate 331 U
50-29-3 4, 4'-DDT 331 IJ
72-43-5 Methoxvcnlor 1656 U
53494-70-5— Endrin ketone— 331 U
5103-71-9 alpha-Ch lor dane 166 U
5103-74-2 gamma-Ch lor dane 166 U
3001-35-2 Toxaphene 3313 U
12674-11-2 Aroclor-1016 1656 U
11104-28-2 Aroc lor-1221 1656 U
11141-16-5 Aroc lor-1232 1656 U
53469-21-9 Aroc lor-1242 1656 LJ
12672-29-6 Aroclor-1248 1656 U
11097-69-1 Aroc lor-1254 3313 U
11096-82-5 Aroc lor-1260 3313 U
FORM 1 PEST 1/37 Rev.
CO o1 U +
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M4A06
Sample Number: 9S182
Operator :
Time
Study
8/30/89 1:56 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89 9:24 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
47.00
1.0
nun.
min.
pts/sec
e:\pkd\MCFR02 8.raw
e:\pkd\MCFR028.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tim* Cooponaat Adjuatad Anount Raw Anount ?aak Araa Paak St MULTIPLIER
(mln) Nana UC/fb UC/)& [uV-sacJ [uV] Adj/Rav
25.36 DBC
117.
.81
170.
. 74
2.27«6
33343.06
0.69
vs
Total Ar«* « 4645640.00
Total Concent radon ¦ 207.3449
Report by Tim Rand, Lockheed-ESC
000105
-------
„ , Chroraatogram
FileMame : e:\pkd\HCFR02B.raw Date: 8/30/09 1:56 PN Page 1 of 1
Start Tine: 0.00 ain End Tiae: 47.00 ain Low Point: -2117657 uV High Point: 956550 uV
Vertical Scale Factor: 0.00 Plot Offaat: 0 altf Plot Scale: 250 mV
DO
DO CO
a a
250.000
208.333
166.667
125.000
83.333
.41.667
-0.000
7.83 15.67 23.50 31.33 39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Nana : M4A06
Sample Number: 9S182
Operator :
Time
Study
8/30/89 2:37 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
9:24 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File
Inj. Volume :
Sample Amount :
e:\pkd\MCFR0 2 8.raw
e:\pkd\MCFR02 8A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
*EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
!Ut Tiaa Caoponaac Adjuacsd Amount Raw Amount P.mk Area P.&k Ht MULTIPLIER
(Bin) Haaa UC'tt* U6/9& tuV-sae] [uV] Ad)/JUw
¦oii» » amawg
•to.at DOB-
25.36 0BC
BIBQCWAM
11 ii aoeosi
t-r&-
?0.5»
iot.e»
.04»6 0*070.00
183 3M98.6I
b9i k9
aa»a> aix»i99
140.76
204.00
2.27«6 53343.06
r*9-
Qit*
0.69
t/fc.
¦/lt-
Total Arta • 4636240.00
Total Concentration ¦ 239.2634
Report by Tim Rand, Lockheed-ESC
000107
-------
Chromatogram
Page 1 of 1
HleNaae : e:\pkd\HCFR02B.rau Date: B/30/B9 2:37 PH
Start Tine: 0.00 ain End Tin: 47.00 ain Low Point: -2117657 uV High Point: 956550 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 mv Plot Scale: 250 mV
CO
250.000-
20B.333-
166.667-
125.000-
83.333-
41.667-
O
o
Q.ooo-
C
QC
Cs CT>
o
ccS
CO
DO CO
in
m ~
i ill
IT
i 'i
vVrr~irr^V
!rr =j=
CD 9
_L •
I
§i e
I I I
I I I I j^T* I i*? I iuT1 l
&
I I I I I T'l I I I i^T* I I I I I I I I I I I I I I I I I » I I I I I I I I
7 . 83
m
mU-5V
t i mp t m i it)
Jl,
-------
Nelson Analytical 2700 Chromatography System Report Header
/ample Name :
Jample Number:
Operator
nter-face #
HutoSampler
J*ack/Vial
M4A06
9S182
5 Channel
None attached
0/0
Time
Study
8/29/89 5:03 PM
MCFARLAND
Jata Acquisition Time#
i
t
e1ay T i ma
n d Ti me
Sampling Rate
taw Data File
eault File
.nstrument File
Vocess File
~ample File
Sequence File
0.00
70.00
1.0
8/29/89 3:02 PM
min.
min.
pts/sec
A/D mV Range
1000
C:\2700\GCS\MCF3026.raw
C:\2700\GC5\MCF5026.rst
C:\2700\GCS\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC3\MCF54A.seq
inj. Volume
Sample Amount
2 uL
1.0000 UG/kg
Area Reject
0.00
loise Threshold
ilution Factor
ivisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
0. 69
0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Splift Ratio
Temperature
I n ,i ec t i on T emp
Detector 1
Detector 2
Notes
VARIAN 3400 ""D
.25MM ID .2SUMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number ot Peaks Detected: 41
BCTERNAL STANDARD REPORT
\et Time
Cmin ]
Component
Name
Adjusted Amount Paak Area Peak Ht Raw Amount
ug\^ CuV-aec] CuV] ugXs.
5-t. 2-7-AkDRIN—
.26.21 HEPEPQX
30.02 CNDQ1
73.07 DICLDPlIN
-30. 19 CNC02
'11.16 ENDALD
-2247. 00-
2077.00
0. 72
-0. 47
-7-730.00-
1401.50
O. 57
oooioa
773. 50-
1 TO —»—
1 %/ii • *- ¦->
-281.33
¦A1
4-25.09
—67.44
-?2.-9
-------
'16. OS DDT 1 *1 19 525151 02 2075. 27 20. 56
55i0l METIIQXV 10.9-1 5944.50- 592.44 15. Ql-
61.37 DBC 162.40 226342.03 19901.02 235.37
Total Area = 276380.56
Total Concentration = 191.1024
Report by Doherty Bresnahan
000110
-------
FileNaae : C:\2700\6C3\HCF302i.raw Data: 8/29/89 3:06 Ptt Pap t of t
Start Tioei 0.00 tin End Tioa> 70.00 ain low Point: 2198 uV High Point: 45492 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Cfcxoiatograft
i t;? s 8 ft ?s It8t 21 a ss *
s ;i> i ri c ug i
-mrrnr'niTi mm hi mi I'm n rmi imi n
K iiiilii e
4—* S, ? h, —L
1111
54.33
11H 23.33 35.09
TIm (aia)
OOOlll
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M4A06
Sample Number: 9S182
Coerator :
T ime
Studv
3/30.-59 3:0-3 AM
MCFARLANC
Inter-face #
AutoSampler
Rack./Vial
5 Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Time: 8/29/39
0.00 m i n.
70.00 min.
1.0 pts/sec
3:02 PM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5026. raw
C:\2700\GC5\MCF5026B.rst
C:\2700\GC5\FOE.ins
C:\2700\SC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
Inj. Volume
Sample Amount
2 uL
1.0000 UG/kq
Area Reiect
V. 00
Noise Thresnold
Dilution Factor
Divisor
1
1. <30
1.0000
Area Thresnold
Mu11 i p11er
Additive Constant
100
0.69
0. 00
Buncfi Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sol it Ratio
T siiiBerature
In.iection Temp
Detector 1
Detector 2
Notes
y'ARIAN 3400
.25MM ID .25UMFILM RTX3
30M
HE
20CM/SEC LINEAR VELCC IT.' 15
160 1/MIN TO 230
200
300
Total Number o-f Peaks Detected!
41
***«
0CTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount Peak Area
A, CuV-sec]
Peak Ht
C LlV ]
Raw Arcant
US'TL
JL ± t
ALPftitj
¦ T'Q
2247.00
132.23
*7 f
i ii 1
— a er .1
r-k^r-
nn'nn 1
i* 'T v U * • » w
... i.. - |
_'W • /
ENDRIN
I™. ti?s
132S^14
1 !3
-» 4 tr
t
000112
1
I
-------
44. oa CUDOGULrftTC &r 1229.00 55. 27
51.04 CNDKCTO 0. .30 455i 00 39. 33 0.44
61.37 DBC 206.32 226342.03 19901.02 299.01
Total Area = 536884.13
Total Concentration = 279.9784
Report by Doherty Bregnahan
ooona
-------
FileNaaa : C:\2700\GC3\HCF3024.ra* Date: 8/30/89 8:49 AH Pigt 1 of 1
Start TiM< 0.00 ain End Tia»» 70.00 ain Lon Point: 51?0 uV High Point: *5*92 uV
Vertical Seals Factor: 0.00 Plat Offset: 0 aV Plot Scale: 100 aV
Chromatogram
*iG
* ; «a t ss k as a ss *t* *
; sa e ri r mi$;s ::»b re its i
i—mi ,iii iimi imn ,11111 mini i'ii! 11 I'nntfnr
« 1 1
n %
II _ i. i 1
•H 8,5 8 *, ,'r
11.67
23.23
35.00
Titt (tin)
#.W
58.33
000114
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
t£PA SAMPLE NO.
M510
Lab Names LQCKHEED-ESC
Contract: 68-03-3249
Lab Code: Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 4.9 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.: SDG No.:
Lab Sample ID: 9S189
Lab File ID:
Date Received: 7-23-89
Date Extracted: 8-1-89
SONC Date Analyzed:
Dilution Factor: 10
CONCENTRATION UNITS:
uq/kg Q
319-84-6
319-85-7
319-36-8
53-89-9
76-44-3
309-00-2
1024-57-3
959-98-8
60-57-1
72-55-9
72-20-8
33213-65-9
72-54-8
1031-07-8
53494-70-5
5103-71-9
5103-74-2
3001-35-2
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-3
aloha-BHC 168 U
beta-BHC 168 U
del ta-BHC 168 U
gamma-BHC (Lindane) 168 U
Heptachlor 168 U
Aldrin 168 U
Heptachlor epoxide 168 U
En dosu 1 -f an I 168 U
Dieldrin- 336 U
4,4' -DDE 336 U
Endrin 336 U
Endosul-fan II 336 U
4,4'-DDD 336 U
Endosul-fan sulfate 336 U
4,4' -DDT ...36 U
Methoxychlor 1682 U
Endrin ketone 336 U
alpha-Chlor dane 163 U
gamma-Chlordane 168 U
Toxaphene 3365 U
Aroclor-1016 1682 U
Aroc lor—1221 1682 U
Aroc lor-1232 1682 U
Aroc lor-1242 1682 U
Aroc lor-1248 1682 U
Aroclor-1234 3365 U
Aroc 1 or-1260— 3365 U
FORM 1 PEST
1/87 Rev.
occI
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface # :
AutoSampler :
Rack/Vial :
M51Q
9S189
Time
Study
8/31/89 3:55 PM
MCFARLAND
2 Channel ; 1 A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
2:46 PM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e:\pkd\MCFR033.raw
e:\pkd\MCFR0 3 3.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 UL
1.0000 UL
Area Reject
; 0.00
* ## * * EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat flat Ceapo&wt Adjuatad Amount Rait Amount P«ak Area Faak Be MULTXfLISt
(mini Hum UC/fA QCltS* (uV-i.e) [uV] AdJfSUu
S.*0 MiDMW
.? »7 mnat
a tt srooi
11.11 BiSfcBIWt
o i at
imia
i,3i ttiiiBi.oa ¦ lain m
. ¦>» 8TS*e.8g 11 t8»8,8»
>3.83
M' lf ' 71 111
a. a a
Ti , 7Qui
¦ lK
¦vC
M.ta iimoa
l*r» 00*
ta.>a ehbalp
rM<
aoTf"»"! o»"
Q7i»t
U.*0
a__ii2A_U-
0"i>8
•M*-
OO.
25.57 0BC
127.78
182.3*
2.43«6 56084.»»
0.76
Total Arc* - 7»30*#2.00
Total Coacaatraclaa " 1*3.MAS
Report by Tim Rand, Lockheed-ESC
sssssssssrsss
000116
-------
Chroraatoqrara
FileUaae : e:\pkd\KCFR033.rau Date: 8/31/89 3:55 PN Page 1 of 1 3
Start Tiae: 0.00 ain End Tiat: 47.00 ain Lou Point: -1247457 uV High Point: 2052270 uV
Vertical Scale Factor: 0.00 Plot OffMt: 0 aV Plot Scale: 250 aAr
250.000-
tsj i—i i*-» KJ
(A «— OO
f-S I—¦ cjrl d
ro m cn o
H~> IT) -a" *—
^ r-J cH —*
— -— -— CN
208.333-
166.667-
cz
CD
CO
a>
125.000-
83.333-
o
o
c
41.667-
-0.000-
-rTTuW'VTT
I I I
^ s 2
S g fcc1
i i i r3!
i i i'
ss
Lf I *pl
i i i r
-P^T
I I I I I
,-C^l
i i n ¦
7.83 15.67 23.50
Time (niin)
31.33 39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : MS10
Sample Number: 9S189
Operator :
Time
Study
8/31/89 4:22 PH
MCFARLAND
Interface #
AutoSampler
Rack/vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : o.oo min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
2:46 PM
Rav Data File
Result File
instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e:\pkd\MCFR03 3.raw
e:\pkd\MCFR033B.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat tiarn Csapenaat Adjtutad Amount Raw mount Paalt ?aak Bt HUITMLXER
lata) Nana UC/Kb [uV-tmcl [uV] Adj/Raw
i. aft MJUlll
i.tn onbD
-------
Chromatogram
FlleNaaw : e:\pkd\MCFR033.raw Date: 8/31/89 4:22 PH Page 1 of 1
Start Tine: 0.00 Bin End Tine: 47.00 "In Lou Point: -1247457 uV High Point: 2052270 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 itt Plot Scale: 250 mV
250.000-
208.333-
166.667-
, S? £5 !£? 63 ~ § C=j
^ «iS K cn o -«r rv cp — Mi «S
rsj cn rg
«C
% /
H
o
o
o
Of
£
o
n
en
125.000-
83.333-
41.667-
-0.000-
T VT TT TTTfTrrf
hi
CD
I
o
V a & 8
t-r>
S
St*
i i nfi i i i j~r i it i i*t i r~j i i i i i i 7—1 i j i it i i i i i i | i i i i i i i i i [ i i i i i i i i i
7.83 15.67 23.50 31.33 39.17
Time (min)
-------
41.21 CNDflLD t-r-94 2606.77 194. .32
16.09 DDT 571 96—05242. 13 7547.20 54.23 #
55.64 MCTHOXY 2839.75 199.05
61.41 DBC 192.39 264312.09 23152.77 274.85
: Qoi
4.23
Total Area = 376523.91
Total Concentration = 245.2377
Report by Doherty Bresnahan
000121
-------
FilaNiaa : C:\2700\6CSVCFS031.rw Data' 8/30/89 7:39 AH Pap 1 of 1
Start Tiati 0.00 tin End Tiaat 70.00 ain Low Point: 3232 uV High Point' 32086 uV
Vertical Seals Factor' 0.00 Plot Offset' 0 nV Plat Scale' 100 aV
Chrotatograa
ltl
* c. s
» »* Si
3
um_l
3
iW-4
5$ ssst; s; ?«*
RiCEKflU**llfcM5 JC ? S aF8 p 118 1IM
I
—m—jsni: iiiiiiirinfrmrtW^Trrr^nrirbr rTrrmnfnrmTi'rf'rTf!! ranrri
t I | I s i a i 6
A * ? , \ %r 1», 3 S L
Mt
11.W a S3 35.00
Tia* (ain)
n.a
S.3J
000122
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : MS10
Sample Number! 9S109
Operator :
Time
Studv
3/30/89 8s 59 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range s 1000
Data Acquisition Time: 8/29/89 10:26 PM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Samp 1e File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC3\MCF3031. raw
C:\2700\GC5\MCFS031A.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCFS4B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject : 0.00
Area Threshold : 100
Multiplier : 0.70
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T emperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400-*5"
.25MM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
15 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 72
**********
EXTERNAL STANDARD REPORT
o.O't -f;
0 i 20 JJ
)d
Ret Time Component Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin] Name ug\ !
-------
¦7b. BO EMPESUI
LLA,
U-Z.
40.35 DDD
1.79
2701
¦ r *.<
1 ?t? r»-i
256.39
SJ
i
44.67 EMOOSULFftTE
-0.47
7<=> 79
5(1, 78 ENOK FTQ
-0-.
306.00
18.27
61.41 DBC
244.42 264312.09 23152.77
349.17
Total Area = 628741.50
Total Concentration = 333.2749
Report by Doherty Bresnahan
000124
-------
FileNue : C:\2700\SC3VCF3031.r« Data: 8/30/89 9:00 AH Pap 1 of 1
Start Tioat 0.00 tin End Tioat 70.00 tin Ion Point: 5232 uV Hi
-------
ID
PESTICIDE ORGAN ICS ANALYSIS DATA SHtET
Lab Names LOCKHEED—ESC Contracts 68—03—3249
£PA SAMPLE NO.
MI 16
Lab Codes Case No. s
Matrixs (soil/water) SOIL
Sample wt/vols 30 grams
Levels (low/med) LOW
V. Moistures not dec. 0.2 dec.
Extract ion s (SepF/Cont/Sonc)
GPC Cleanups (Y/N) Y pHs
CAS NO.
COMPOUND
SAS No. s SDG No. s
Lab Sample IDs 9S195
Lab File IDs
Date Received! 7-25-89
Date Extracted! 8-1-99
50NC Date Analvseds :"i
Dilution Factors 10
C CNCEN I"PAT I CM UN IT3:
ka 0
319-84—6
319-85-7
319-86-8
5S-89-9
76-44-8
309-00-2
1024-57-3
959-98-8
60-57-1
33213-65-9
72-54-8
1031-07-8
50-29-3
72-43-5
53494-70-5
5103-71-9
5103-74-2
8001-35-2
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
-alPha-BHC
-beta-BHC
-delta-BHC
-gamma-BHC (Lindane)
-Hep tach 1 or
-A 1 dr in-
-Heptachlor epoxide
-Endosul-fan I
-Dieldr in
-4,4'-DDE
-Endrin
-tndosu. 1 tan I I
¦4.4'-DDD
-Endosul fan suit*ate
-4.4'-DDT
-Methoxych lot 1
-Endrin ketone
-alpha-Chlordane
-gamma-Ch1or dane
-Toxaphene 3
-Aroc lor-1016 1
-Aroc lor-1221 1
-Aroc lor-1232 1
-Aroc lor-1242 1
-Aroc lor-1248 1
-Aroc 1 Gr- 1254 3
-Aroclcr-1260 3
160
160
160
160
160
160
160
1 oO
321
321
321
321
321
603
321
160
160
206
603
603
603
603
603
206
206
U
u
u
u
L)
U
U
U
u
u
I I
u
u
u
u
u
u
u
u
u
u
u
u
FORM 1 PEST
Z-CGiJU*
1/87 Rev.
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : N116
Sample Number: 9S195
operator :
Time
Study
8/31/89 4:09 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 ¦ Channel : S A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
8:46 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR04 0.raw
e:\pkd\MCFR040.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 0.00
~~~~~EXTERNAL STANDARD REPORT"^
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
Iain!
Coapaaa&e
Adjuatad Mount Saw Amount PaaJt Araa
!uV""e>
Paak Be MULTIPLIER
(uV) A4)ffUw
onrnpow
¦»,m Etmoi
4
is it iima
-t>isa dm
23.5* DBC
t.li
aa.i*
¦a.n tvit.6*
3>6». *9
»8i6I OlOOOO.gB—1i>6*
191.11
i»"i so-
ui. ua i.2B»g 1JJJ8/.W
n.J« Jiana.aa maau.ft
!!»¦¦»•
Wt-
n»ia»
e.asag na*«
-»rW— 1101 ¦ a*
128.as
192.01
2.Stmt S690i.20
j . o i
""T rwr
0.6T-
o.tJ
-ic
-Mt-
Total Araa - 9918290.00
Total Coneaatratloa • *17.k90S
Report by Tim Rand, Lockheed-ESC
CCO!'^
-------
Mil Mite
250.000-
S K SBf^PS b=5 ^ £?;s & JS
~H >o CP C> cJ TT r—.* ct* ^-' «r-l >-} wS
C—I CN t»
208.333-
166.667-
cn
Cki
125.000-
83.333-
41.667-
-0.000-
-nrr^!
r^ri
i T* i fn i i i f-f i Ft T11 i i i i | i i "r* r*f i i i i | i » i i i i i i i | i i i i i i i i i
7 .83
15.67
39. 17
23.50
Time (min)
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : N116
Sample Number: 9S195
Operator :
Time
Study
8/31/89 4:35 PM
MCFARLAND
interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
8:46 FM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e:\pkd\MCFR040.raw
e:\pkd\MCFR04 0A.rst
e:\pkd\pkd. ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRIUD.seq
2 uL
1.0000 UL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
ssaasssssssssssssss
Rtt turn Ceopaatac Adjusted teowc Rav Aoouac P««k Aril ?««k He MULXXFLXSL
[nla] Hum UC/^ [uV-a«o| [uV] AdJ/IUv
-V
23.36 DSC
lit.
VK
133. n
129.*2
2.SS.6 36906.20
0,6?
Total Ana - 7S37«S1.00
Total Concentration • 3*J.*7*3
Report by Tim Rand, Lockheed-ESC
OCO(2Ci
-------
, „ ' Chromatogram
FileMaae : e:\pkd\MCFRMO.rau Date: B/J1/B9 4:16 PH Page 1 of 1 ^
Start Tine: 0.00 ain End liae: 47.00 nin Lou Point: -1541917 uV High Point: 2069250 uV
Vertical Scale Factor: 0.00 Plot Offaet: 0 nW Plot Scale: 250
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : N116
Sample Number: 9S195
Operator :
T ime
Study
8/30/89 3J 21 AM
MCFARLAND
Inter-face # : 5
AutoSampler : None
Rack/Vial : 0/0
Channel
attached
A/D mV Range : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
I n j. v'o 1 ume
Sample Amount
T ime»
0.00
70.00
1.0
8/30/89
min.
min.
pts/sec
7:06 AM
C:\2700\GC5\MCF503S.raw
C:\2700\GC5\MCF3038.rst
C:\2700\GC5\F0E.ins
C:\2700\QC5\EXSTD.pre
C:\2700\GCS\MCFS1A.smp
C:\2700\GC3\MCF34A.seq
2 uL
1.0000 UG/kg
Area Reject
: 0.00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
0.67
0.00
Bunch Factor:
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sp1i t Rat io
T emperatare
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 13 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 90
it *********
EXTERNAL STANDARD REPORT
Ret Time
[ min 3
Component
Name
Adjusted Amount Peak Area
ug\^> EuV-sec]
Peak Ht
CuV3
Raw Amoun t
uq\L
30.13 CND01
33.09 D ID-DP IN
~a.a0 SMD03
12.313 G-BHG
"M ALDPTN
0.-42-
—3555.00
"r23 '~w">
—-533»63
0 i63 t
•"¦a i
2 HEPEPOX
0. 21
359.99
50.15
0.31
-4-rSS 337,. 91
9.61 20395. 00 1472. 63-
635 y-55~
COC i 3
1/
-------
401 80
ENDrtLD
1 Q1OO
22575.75
2 3. 9'i)
-SS.S7
METHQXY
1.39
¦ 'J3
2363.00
117.17
»t-44
61.40 DBC 166.62 239149.00 21711.74 248.68
I
f
Total Area = 553647.13
Total Concentration = 308.1285
Report by Doherty Bresnahan
-aeetw—
L CC I y —
-------
FileNaaa : C:\2700\GCS\t1CF5038.rM Data* 8/30/89 8:22 AH Pas* 1 of 1
Start Tiw< 0.00 ain End TiM> 70.00 nin Low Point: S242 uV High Paint: 67740 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 nV Plat Seals: 100
Chmatograx
INI
ft & gg.aSSS ffSSlS X. SSSSfiXfC 33* 3 = «5
3 *9 555? ::&2 k cftansKAit a aiBb
I i I f I M
11.(7 23.33 35.00
Tin (lin)
53.33
-009^
C CO iB-S
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : N116
Sample Numbers 9S195
Operator :
Time
Study
8/30/39 9:16 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/0 mV Range : 1000
Data Acquisition Times 8/30/89 7:06 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
I ri ,i. v'o 1 ume
Sample Amount
0.00
70. 00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5038. raw
C:\2700\GC5\MCF5038A.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 US/kq
Area Reject
J 0.00
Noiss Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
0.67
0.00
Bunch Factor:
Instrument Conditions
Capillary GC -
I nstrument
Column
Column Length
Carrier Gas
Flow Rate
So 1 it Rat io
temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400-5
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
160 1/MIN TO 230
200
300
13
Total Number of Peaks Detected? 90
Ret Time
[ m i n J
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
u<3 C uV-sec D
Peak Ht
CuV]
Raw Amount
uq\L
75 A DI1C
-S3 B-BHG
1' '1.56 D-3HC
it. 30 ftLDRIN-
-o ,11 r-pmi naiMF
30.99 A-CHLDAME
Q. 07
15?.61
i555.00-
0. 44 25-75.92
O'J
-176.10
-50.56
5-55. 00
0. 66 3343^59 272. 77
0. 75
COO 13^
-ZQ&y-.-22-
-£03. 00
^ o£-
0. 08
0. ?'?
¦1. ts
I
-------
•M.57 OPS OS. b 377570.00—.2126. 00
¦
V*1
= (\
EMQR uL .. .
.. -S-LQ.
-> 7i
- 6664.-63
nr ->g
. -421-
.38
7
-^i|
c-Kinnei n SAtff
1 69
:1595 rt2
29^
96
ENDK€T0
9. 42
114.3.
r-±S
1r4.
r£<®.
61.40 DBC 211.67 239149.00 21711.74 313.93
Total Area = 669772.73
Total Concentration — 324.5028
Report by Doherty Bresnahan
3^
JOO
Ceo 13 S"~
-------
FileNut : C:\2700\GC3\rtJ5038.rat. Dats: 9/30/89 9:17 AH Pag* 1 of 1
Start Tin! 0.00 ain End Tinas 70.00 ain Low Point: 5242 uV High Point: 67940 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 «V Plot Seals' 100 aV
Chraaatograi
INI
k k (| !• SS5 8 C 8 !| 8 J •!33SIS" 3S! % ISSR^ 9-}!|
- 3 +2S2Z 5 SsRX R CSxtlAMPill 555 CSSlB f<* fife* 8 828ft
|
II
n
5
1(1X7-3
11.W 23.33 35.00 H.U 58.33
TiM (ain)
-QWISOon
ocorit.
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
t£PA SAMPLE NO.
OFOl F'REGPC
Lab Name: LQCKHEED-ESC
Contract: 63-03-3249
Lab Cade: Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
Moisture: not dec. 1.9 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) N pH:
CAS NO.
COMPOUND
SAS No. : — SDG No. s
Lab Sample ID: 9S177
Lab File ID:
Date Received: 7-25-89
Date Extracted: 7-31-89
SONC Date Analysed: &'3C'%"ci
Dilution Factor: 10
CONCENTRATION UNITS:
ug/kg Q
319-34-6 alpha-BHC 32 U
319-35-7 beta-BHC 32 U
319-36-3 del ta-BHC 32 U
58-89-9 qamma-BHC (Lindane* 32 U
76-44-8 Heptachlor 32 U
309-00-2 Aldrin — 82 U
1024-57-3 Heptachlor epoxide 92 U
959-98-8 Endosu 1 fan I 32 U
60-57-1 Dieldrin 163 U
72-55-9 4, 4'-DDE 163 U
72-20-8 Endrin 163 U
33213-65-9 Endosu 1 fan II 163 U
72-54-8 4,4' -DDD 163 U
1031-07-8 Endosulfan sulfate 163 U
50-29-3 4, 4'-DDT icZ U
72-43-5 Methoxychlot 315 LI
5-494-70-5 Endrin ketone 1j3 'J
5103-71-9 alpha-Ch lor dane 32 U
5103-74-2 gamma-Ch lor dane 32 U
3001-35-2 Toxapnene o 31 U
12674-11-2 Aroclor-1016 315 U
11104-28-2 Aroc lor-1221 ' 315 U
11141-16-5 Aroclor-1232 315 U
53469-21-9 Aroc lor-1242 315 U
12672-29-6 Aroc lor-1248 815 U
11097-69-1 Aroc lor-1254 1631 U
11096-82-5 Aroc lor-1260 1631 U
FORM 1 PEST 1/37 Rev.
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : OFOl Pre-GPC
Sample Number: 9S177
Operator :
Time
Study
8/30/89 1:36 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
4:14 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR0 2 2.raw
e:\pkd\MCFR0 2 2.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 UL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rae Tin
total
Coopooanc
Adjuacad /Amounc Raw Amount Paak Araa Paak Be MULTIPLIER
UG UC/L [uV-i«c| (uV] Adj/Raw
iittchlh
ALDRIW
-iS.SS-£WK»
47.«» BBt
25.73 DBC
a. tii
1 mi6(i rm '¦««¦» •»«
—13900 ¦ 00
73. W -
0.*8
107.4 3
9^4-
19810.75
013.90
saa.t?
27.07
137.29
39.oa a>9*sa.aa oaa».7*
201.90
2.69a« 61822.AO
-9t-68-
. <*»
. f.v»
a.jg
0.00
3.68
Total Araa • 5*12498.00
Total Coocantcatian » 238.9328
Report by Tim Rand, Lockheed-ESC
jQQQ122-&3
qOO(3?
-------
Chromatog ram
FileNaae : e:\pfcd\HCFR022.raw Date: 8/30/S9 1:36 PH Page 1 of 1
Start Tine: 0.00 ain End Tiao: 47.00 as in Low Point: 4700 uV High Point: 70*890 uV
Vertical Scale Factor: 0.00 Plot OfUet: 0 bW Plot Scale: 250 atl
250.000
208.313
166.667
125.000
CO
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number:
Operator
Interface #
AutoSampler
Rack/Vial
OFOl Pre-GPC
9S177
Time
Study
8/30/89 2:24 PM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
4:14 AM
Raw Data File :
Result File
Instrument File:
Process File
Sample File :
Sequence File
Inj. Volume
Sample Amount :
e:\pkd\MCFR022.raw
e:\pkd\MCFR0 2 2A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Rat Tlaa
[mini
Caopeaaac
Adjtucad Amount Raw Amount P«*k Ax*> Pafck He MULTIPLIER
».«» B BH0
i.tg ALD1UM
0»:65~
UC/L
(uV-««c)
[uV]
AdJ/Raw
-UK"
ODfl
-13.63 ODD
25.73 DBC
—o.3a—
on—
-frrW—20960.00 1368.89
0.36-
-0.26 5390,00 350.15-
17
- -O-HW-
23.1fr-
164.04
110.
- 1.20 10010.73
33.96 906136.06
241.23
320.6?
5163.30
2.69«6 61822.60
0. 00
: ^
i ^
0.60
0.60
-Or^fl t^iS
0.68
Total Ar«& • 5383488.00
Total Concentration • 268.3824
Report by Tim Rand, Lockheed-ESC
oooiaa-^a
CQO110
-------
Chromatogram
FileNaoe : e:\pkd\HCFR022.raw Date: 8/30/89 2:24 PM Page 1 of 1
Start lias: 0.00 ain End Tiae: 47.00 ain Low Point: 4700 uV High Point: 704890 tN
Vertical Scale Factor: 0.00 plot Offset: 0 oV Plot Scale: 2S0 mV
c=
o
cd.
CO
«X»
o
o
c
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
—4 o CTt
2 ^ ^
2
U-> Cm
li> CO
iri r~»*
CM
Vnr.T
»—rrr
• -|
c_> o
o
I
it S
LO
S
i *Pi i i i i i*? i i*Y i Fj i i i i i i T*1! i | i i? i i i i i i j i i i i i i i i i j i i i i i i i i
7 . 83
15. 67
23 . 50
Time (min)
31.33
39. 17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
Inter-face #
AutoSampier
Rack/Via j.
OFOl pre-gpc
9S177
5 Channel
None attached
O/O
Time
Study
8/29/89 10:14 AM
MCFARLAND
A/D mV Ranqe : 1000
Data Acquisition Time« 8/29/89 7:37 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
0. 00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5015E. raw
C:\2700\GC5\MCF5015G. rst
C:\2700\GC5\F0E.ins
C:\270O\GC5\EXSTD. pre
C:\2700\GCS\MCF51A.smp
C:\2700\GC5\MCF54A. seq
In .j,
Volume
Sample Amount
Noise Thresnold
Dilution Factor
Divisor
2 uL
1.0000 US/kg
1
1.00
1.0000
Area Re-sen • 0.00
Area Thresnold : 100
Mul t ip 1 ier :' 0. 63
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow n-i.ts
Split Ratio
T SiTparaturs
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400—5"
.25MM ID .25UMFILM RTXS
30M
HE
20CM/SEC LINEAR VEL0CIT
160 1/MIN TO 230
200
300
15 PS I
Total Number o-f Peaks Detected: 42
Ret Time
Cmin 3
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount
ug-vC c
Peak Are*
CuV-sec 3
Peak Ht
CuV3
Raw Amoun t
ua \L
10. *75 HPTC1ILR
-ts-
437.00
604'?. 00
o. n3
1.4h
I
-a-1.25 ALDHlIH
27.05 IICPEPQX
9iLi
17
-3S-
320.42
712-.0O 5-2-.-9S-
1342. 50 T~ ~
30.10 ENPQ1
33.93 DIELDHIN
30.15 CN001
80S.00
i.... j
5S. a4
-•>-.-23-
7 64.00
52. o:
000131-t^
OCOI*^
0.01
. 4
-------
—40. 73 ENDALD - S*-£S 2859.00 261.02 3.01 *^
16.00 DDT —37*75757 ZS557ST" SO.aa ^
554 04 HCTI IOXY 3t4« 1846.00 115.91 5-g 00- **
61.33 DBC 164.. 10 232072.00 18086.73 241.32
Total Area => 279346. 19
Total Concentration = 185.8399
saaaasaasssssssasssaaaaaaaassasssssBsssessssaasssaasssass
Report by Doherty Bresnahan
QQ0132
6^-6 ' *-/ i
-------
FileNua : C:\2700\SC3\nCF301SE.rati Data: 8/29/89 10:13 All Pa« 1 of 1
Start Tiatt 0.00 ain End Tiati 70.00 ain Low Point: 51*4 uV High Point: 28034 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
ChroMtogTU
sag* 53 9SS53*S8S Sis?9 * g t s )i ^ ; S
- >< 3k jss u xaa b n*in: 3 : 0 tc u i 1
I
u
It
s
3
15557-3
1 ik
3-iV-rr*-
t»41
i
i I
i—L
II illlll
u
iiiiili n 11 iiaiii'im
s *
» ¦
.t 1 w
1U7
a.® n.a
Tii* (aia)
58.3
000133
ccom
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : OFOl
Sample Numbers 9S177
Operator :
T ime
Study
8/29/89 2:09 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time* 8/29/89 7:37 AM
Delay Tims
End Time
Sampling Rate
0. 00
70.00
1.0
min.
min.
pts/sec
Raw Data File
Result File
C:\2700\GC5\MCF5015E. raw
C:\2700\GC5\MCF5015K. rst
Instrument File: C:\2700\GC5\F0E.ins
Process File
Sample File
Sequence File
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
In.i. Volume
Sample Amount
2 uL
1.0000 UG/kg
Area Reject
: 0. 00
Noise Threshold
Dilution Factor
Divisor
I
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
too
0.68
0. 00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
3p 1 i t Rat io
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 42
Ret Time
Cmin ]
**********
Component
Name
EXTERNAL STANDARD REPORT
-t-l .-56 B-BHC
13.60 D 01IC ¦ ¦
11.25 ALDRIN
Adjusted Amount Peak Area
UW IL
£/
-rr
•> -%-f ¦
CuV-sec]
Peak Ht
CuV]
Raw Amount
ug\L
040.50
2t
1052.99-
68.94
30.99
0.54
¦ t/H
. l.*l
O.13—
1.50-
-l-r*2 6049. 00
-*>r09-
320.42
20.94 0 CIILDANC
30.92 A CIILDANC
^-29. 00
700.00
42.60
60.67
0. 16
63.77 237230.00 22390.17
— {.4S
JO
0. 23
r4.Cil DDE
eeottrr"©
OOC 1-f S"
Vb.
-------
•361 06
CNDniN
0 ¦ So
6Q6i WJ
6oi64
in
0. 70
a n-r
.it a a
1 A
< /I Crt -r 4
. e- f
61.38
DBC
208.48
232072.00
18086.73
306.58
Total Area = 546144.50
Total Concentration = 287.5825
Report by Doherty Bresnahan
eeetaso-i
CCO I Y6-
-------
FileNua ' C:\2700\GC5\flCF5012E.ru Oat»: 8/29/89 2:10 PH Pag* 1 oi 1
Start Tioai 0.00 ain End Tim 70.00 ain Loh Point: 5144 uV High Point: 3)034 uV
Vertical Seals Factor: 0.00 Plat Offset: 0 aV Plat Scale: 100 uV
ChxoBatograa
, • «•«**>» * Jj 3
x b ua a nmnvz s
i
u
I
tt
41
is.w-3
LA
ta|_ti'T7n—mr
111? 23.33 33.00 5iB
TiM (tin)
COO I ^'r-
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
0802
Lab Name: LQCKHEED-ESC
Contract: 68-03-3249
Lab Code: Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 4.9 dec.
Extraction: (SepF/Cont/Sonc) SQNC
GF'C Cleanup: Y pH:
CAS NO.
COMPOUND
SAS No.: 3DG No.:
Lab Sample ID: 9S178
Lab File ID:
Date Received: 7-23-89
Date Extracted: 7-31-89
Date Analyzed:
Dilution Factor: 10
CONCENTRATION UNITS:
ug/kg Q
319-84-6
319-85-7
319-86-8
76-44-8
309-00-2
1024-57-3—
959-98-8
60-57-1
72-55-9
72-20-8
33213-65-9-
72-54-8
1031-07-8—
"2-43-5
53494-70-5-
5103-71-9—
5103-74-2—
3001-35-2—
12674-11-2-
11104-28-2-
11141-16-5-
53469-21-9-
12672-29-6-
11097-69-1-
11096-82-5-
a 1pha-BHC 168
beta-BHC 163
delta-BHC 163
gamma-BHC (Lindane) 163
Hep tach 1 or 163
A1 dr in 168
Hep tach lor epoxide 168
Endosul -fan I 168
D ie 1 dr in 536
4, 4' -DDE 336
Endrin -536
Endosul-fan II 336
4, 4'-ODD •-"•36
¦Endosul fan sulfate 336
"i,4'-DDT .'36
'f1etho:;ycn lor— — 1=32
Endrin ketone --36
•alpha-Ch lor dane 168
•gamma-Chlordane 168
¦Toxaphene 3365
Aroclor-1016 1682
¦Aroc lor-1221 1682
•Aroc lor-1232 1632
¦Aroc lor—1242 1682
¦Aroc lor-1248 1632
¦Aroc lor-1254 3365
¦Aroc lor-1260 J365
U
U
U
U
u
u
u
IJ
u
IJ
u
u
u
u
u
u
IJ
u
u
u
u
u
u
FORM 1 PEST
1/87 Rev.
cco f4£
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface #
AutoSampler
Rack/Vial
0802
9S178
Time
Study
8/30/89 1:46 PM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
5:58 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR024.raw
e:\pkd\MCFR0 2 4.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
R«e Tlo* Co^eMst
Coin] Ksm
Adjuatad Amount Raw Amount
UC/L UG/L
Peak Ar«a
(uV-i«c|
Paak Be
tu»]
MULTIPLIER
Adj/Raw
25.66.0BC
100.S3
1*4.0*
1.92a6
*4141.24
0.70
V/-
Total Aria - 3298281.00
Total Concentration " 134.9016
Report by Tim Rand, Lockheed-ESC
0COW
-------
FileNaoe : e:\pfcd\MCFR024.raw Date: 8/30/89 1:46 PM Page 1 of 1
Start Tlae: 0.00 ain End Mae: 47.00 ain Lou Point: -1810287 uV High Point: 669870 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale; 250 cnV
250.000
208.333
166.667
125.000
CO
Ck£
83.333
O
O
O
( 2*1.667
-0.000
3
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number:
Operator
Interface #
AutoSampler
Rack/Vial
0802
9S178
Time
Study
8/30/89 2:27 PM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
5:58 AM
Rav Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR02 4.raw
e:\pkd\MCFR024A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rac Tim*
(Bin]
Coapoatat
>>¦«» BBB
u.ta DiiBaaumnB
25>66 DBC
Adjuacad Amount Raw Amount Paak Araa
UC/L UG/L [uV-aac]
Paak Ht
tuV]
MULTIPLIER
AdJ/Raw
-Trr~
¦ lo.ia
63
or
laise
rtl
13 ill
120.47
11.19 1IIIH.M iW.M
172.10 1.92a6 44143.24
8. >»
0.70
%-
Total Araa • 3896*37.00
Total Concentration - 198.333*
Report by Tim Rand, Lockheed-ESC
000140
CCOISI
-------
Chromatoqram
FlleUaae : e:\pkd\MCFR024.rau Date: 8/30/89 2:27 PH Page 1 of 1 7
Start liae: 0.00 ain End Itae: 47.00 ain Lou Point: -1810287 titf High Point: 669870 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 250 nV
Oj
CO
Oct
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
.000-
ro o o ki p^.
2 3 S93 5 5 S
• • • • i
O CD
•— V »£»
cn os rs
An.^n^r-r^
' I I
i i 1*1 *r\ i i i |T i inr i i Fj i i i i i i T*i r i i i^P i i i i i i | i i i i i i
i • ¦
7.83
15.67
23 . 50
39. 17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : 0802
Sample Number: 9S17S
Operator :
Time
Study
a/29/89 12:01 F'M
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Ranqe : 1000
Data Acquisition Timet 8/29/89 10<05 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5022.raw
C:\2700\GC3\MCF3022.rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
Inj. Volume : 2 uL
Sample Amount : 1.0000
Noise Threshold: 1
Dilution Factor: 1.00'
D i v i sor •' 1. 0000
UG/kg
Area Reject : 0.00
Area Threshold '• 100
Multiplier : 0.70
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T emperature
Injection Teinp.
Detector 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
F S I
160
200
300
1/MIN TO 230
Total Number a-f Peaks Detected: 43
EXTERNAL STANDARD REPORT
»***
Ret Time Component Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin] Name ug\L CuV-sec] CuV] ug\L
12. 1" G-BHC <186.50 64.23 OjI-W^
>21.25 ALDRIN 0. 37 2274 . 00 145.60 0.5"
'26.17 HEPEFOX 6236. 00 332. 42 2.22
29. ^ CNDQ1 7.21 27169.50 2000¦ 65 10.30
33.53 0 ID-DP IN 1--3B-—-2793.00 262.63 1. 76 iM
¦=0.26 CND02 0. 50 1627.04 00.01
000142^
COO / S3
-------
I
,1 £5*
CMDALD
11.75..
1579a,61
—1-30.3.6?
161 7 6
4 -re
i fn < 1
w w 1 ^ U
61.33
DBC
125•£>3
172594.00
1.2343.98
179.47
Total Area = 248132.13
Total Concentration = 139.5630
Report by Doherty Bresnahan
_0©(H43^
Ceo i ^
-------
Fileftw : C:\2700\EC3\MCF3022. r» Data: 8/29/89 12:02 PH Pi;* 1 of 1
Start Tiaai 0.00 ain End Timi 70.00 ain Ion Point: 5061 uV High Point: 411299 uV
Vertical Seal* Factor: 0.00 Plat 0«*t: 0 «V Plot Scala: 100 aV
Chroutogru
5
u
41
Ql
UWH
tun—=
sw-j
5WH
II.®-:
34-=
'nrr
% ? s ? ft =5 ts
B S iGII&KaRMM; :: !!R I t li i I
mrniMiiifoniirttia mfii mil 11 w a nfm
i 1 § 1 11
& i i f, i i r. . Y. ¦ it i r.
JLjl
1LW 8,8 3.00
Til* (tin)
58.33
ooo IS^~
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : 0802
Sample Numbers 9S173
Operator :
Time
Studv
8/29/89 2:23 F'M
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attacned
0/0
A/D mV Ranqe : 1000
Data Acquisition Times 8/29/89 10:05 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument Fil<
Process File
Sample File
Sequence File
0.00
70.00
1.0
mm.
m in.
pts/sec
C!\2700\GC5\MCF5022.raw
C:\2700\GC5\MCF5022A.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GCS\MCF51B. smp
C:\2700\GC5\MCF54B. seq
Inj. Volume
5 amp 1e Amoun t
2 uL
1.0000 UG/kq
Area Reject
: 0.00
Noise Threshold
Dilution Factor
Divi sor
t
1. 00
1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
0. 70
0. 00
Buncn Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
'2c 1 i t Ratio
Temperature
I n .1 ec t i on T ernp
Detector 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .23UMFILM RTX3
30M
HE
20CM/SEC LINEAR VELOCITY 13 PS I
160 1/MIN TO 230
2(30
300
Total Number o-f Peaks Detected! 49
EXTERNAL STANDARD REPORT
Ret Time
Cminl
Component
Name
Adjusted Amount Peak Area Peak Ht Raw Amount
ug\L CuV-sec] CuV] ug\L
¦12. 4«>
0 DUG
Igfc.Stt
64.2Z
Q. Z I
iA'
1 •
cc
13.10-
AT 1 HS /.T.
1 E
/• /r
•tO ffiC
i/tr.
*7 C L.
¦¦ / / ju i • yu-
36.70
CNDftIN
1. 26
1577.23
74 . i'*i^
1. 90
009*4536
OGGi^
I
II •
I
-------
40. 26
26.17
596051 56
—2604.06
57.59 ?
61 • wO
DBC
159.61
172594.00
13543.98
228.01
Total Area = 393477.44
Total Concentration = 226.0109
Report by Ooherty Bresnahan
Q0Q146 '¦«
6 CO )
-------
FileNaaa : C:\2700\SC3\f1CF3022. rw Data: 0/29/89 2:23 PM Paw 1 ofl
Start Tiatt 0.00 ain End Tiaes 70.00 ain Low Point: 3061 uV High Point: 411299 uV
Vertical Scala Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Chroiatogra*
5 S RXIK KSRRXM
n.a a a 33.00 #.w a.*
Tia* (ain)
-e6e±4T#>
COO /S?
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
fcFA SAMPLE NO.
P715
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Code: Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
V. Moisture: not dec. 0.7 dec.
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:———— SDG No.:
Lab Sample ID: 9S194
Lab File ID:
Date Received: 7-25-89
Date Extracted: 8-1-89
Date Analyzed: *9'3c-&ci
Dilution Factor: 10
CONCENTRATION UNITS:
ug/kg Q
319-84-6
319-85-7
319-86-8
58-89-9
76-44-8
309-00-2
1024-57-3
959-98-8
60-57-1
72-55-9
72-20-8
33213-65-9
72-54-8
1031-07-8
53494-70-5
5103-71-9
5103-74-2
8001-35-2
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
-a lpha-BHC 161 U
-beta-BHC 161 U
-delta-BHC 161 U
-gamma-BHC (Lindane) 161 U
-Heptachloi 161 U
-Aldrin 161 U
-Heptachlor epoxide 161 U
-Endosul -fan I 161 U
-Dieldrin 322 U
-4,4'-DDE 322 U
-Endrin 322 U
-Endosul-fan II 322 U
-4,4'-DDD : 322 U
-Endosul-fan sul+'ate 322 U
-4.4'-DDT 322 U
-Methoxychlof 1611 'J
-Endrin ketone 322 U
-alpha—Ch lor dan e 161 U
-gamma-Ch 1 or dane 161 U
-Toxaphene 3223 U
-Aroclor-1016 1611 U
-Aroc lor-1221 1611 U
-Aroc lor-1232 1611 U
-Aroc lor-1242 1611 U
-Aroclor-1248 1611 U
-Aroc lor-1254 3223 U
-Aroc lor-1260 3223 U
FORM 1 PEST
1/87 Rev,
oco<±'ci
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface # :
AutoSampler :
Rack/Vial :
P715
9S194
Time
Study
8/31/89 4:07 PM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
7:55 PM
Raw Data File
Result File
Instrument File:
Process File
Sample File
Sequence File
inj. Volume
Sample Amount
e:\pkd\MCFR039.raw
e:\pkd\MCFR0 3 9.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
0.00
~EXTERNAL- STANDARD REPORT*****
Instrument ID: varian 3400-1 GC Column ID: 2250/2401
Rat Tlaa
(mini
AdJujtad Amount Raw Amount Paak Aria Peak He MULTIPLIER
UOltjk. UC fjtfc [uV-aae) [uV] AdJfRaw
1.1 3i llfiTSBtfl
>1 HCTPO*
q»aa amat
H nmMTB
Hi 89 BIBQ»
ni»> aai
23.33 0BC
lit'
a.aa iaat8i»8
1.08
i.it
a¦ fia ooaoie
aaa ¦»
Hita
uni.
ta.aa
j.( hi aa
" 134.30
as.
wa.oe
-MM
.ailTBl.i
>>.aa atan.a
200.73
2.67a6 61366.1
r«-
i.ar
3.BT
a.ta
0.61
0.67
— vt
—i»c
— UC
¦\»c
—
— v*.
Total Acaa - 12836999.00
Total ConctacrftClon • 515.3456
Report by Tim Rand, Lockheed-ESC
CccIO
-------
Chromatogram
FileNaoe : e:\pkd\MCFR039.raw Date: 8/31/89 4:07 PH Page 1 of 1
Start Km: 0.00 ain End lias: 47.00 sin Low Point: -1558947 uV High Point: 1927010 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 bW Plot Scale: 250 mV
250.000
208.333
166.667
125.000
13.333
rr~
-0.000
£3
7.83 15.67 23.50 31.33 39.17
Time (min)
-------
Sample Name : P715
Sample Number: 9S194
Operator :
Nelson Analytical 2700 Chromatography System Report Header
4:33 PM
Time
Study
8/31/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
7:55 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR039.raw
e:\pkd\MCFR03 9A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
~EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
R«t flat Coapoamt Adjusted Aaotmt Raw Aaeusc Peak Ar«« P««k Be MULTIPLIER
(ffllA) Nam UC/JCJjfc UG'f/k (uV-.«c| [uV] Adj/SUv
GfHiPAltD ¦
ift.at m
II 39 PPP
&TF
DirPCCVbTAgB
25.55 0BC
0.0*
ia?i
!» M
369.»9
• a,n mi t\ aa atattia?
aa.a«
160.70
m
239.85 2.67*6
»0
61366.10
8.67
J i <11
-l/K-
-M-
0.6* iS
0.67
Total Arta • 11475921.00
Total Coaeaatratloa ¦ 475.4975
Report by Tim Rand, Lockheed-ESC
CCOI^
-------
Chroroatograra
FileUaae : e:\pkd\HCFR039.rau Date: 8/31/89 4:33 PM Page 1 of 1 ^
Start Tiaes 0.00 ain End Tias: 47.00 ain Low Point: -1558947 uV Nigh Point: 1927010 uV
Vertical Scale factor: 0.00 Plot Offset: 0 «V Plot Scale: 250 oV
u->
m
oO
250.000
208.333
166.667
125.000
41.667
rr
-0.000
CJ
7.83 15.67 23.50 31.33 39.17
Time (rain)
-------
Sample Name
Sample Number
Operator
Inter-face #
AutoSampler
Rack/Vial
Nelson Analytical 2700 Chromatography System Report Header
P713
9S194
5 Channel
None attached
0/0
Time
Study
8/30/89 8:16 AM
MCFARLAND
A/D mV Range
1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
Timet 8/30/89 5:52 AM
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5037.raw
C:\2700\GC3\MCF5037.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Re .1 ec t : 0. 00
Area Threshold : 100
Multiplier : 0.67
Additive Constant: 0.00
iunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
5pIi t Ratio
Tamper ature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400-S"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 13 P3I
160
200
300
1/MIN TO 230
Total Number af Peaks Detected: 68
~
Ret Time
C m i n 1
rnttt
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
uq \ .!$a. CuV-sec 3
Peak Ht
iuV]
Raw Amount
uq\L
frS.42 (3-BHC
flLBRIN
4 HSP'EPQX
HQ. 2.1 EMD01
53.91 DIELDRIN-
*3,
s.mdo:
-ii.
MM. 23
112.-8
It. 10 90271.50
-a®
. m •
'<7» 1Q
-^=r >$$£.
21.04
- 'jr^H
4-504.50
131.OS
-l-w-OO-
3918.00
137.10
I. -19
Qooisa-^
OGCIW
3". €*5 o 43^i i 37
9157.00
500.00
). S3
AIS.67
-4th
f
I
-------
ENDrtLO
17.90
2D2Q7.00
1763.02
26. 34*
MCTUnY V
¦? 38
« OTA ,-,/1
19'ltel • 1 J
1 A £. AO
61. 40
DBC
194.44
279087.00
24029.09
290.21
ooi
is>
Total Area = 592509.25
Total Concentration = 311.3402
Report by Doherty Bresnahan
C'C 0
-------
FilaNtM : C:\2700\GCS\MCF5037.rw Date: 8/30/89 8:16 AN Pag* 1 oi I
Start Tioat 0.00 ain End Tiw* 70.00 nin Lot* Point: 5249 uV Hiah Point: 806661 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 uV
Chromatograi
5
a
U
%
INI
« a *3 s ft* 3*?ca esftS mc
* 3 • 9 B 5S SZ S KR CffRA * «»« CSJS 7a C R Kl I fi >86
501
I ,
H'H^irnniiiini mil i m i 111iff'rrr^rrrr'rrrnWrrriii; n:: u n' i'! iiiiit
* j i I a I j|
.'I I I ¦ I*. I ?i I I "i I r. I ?l . it I Hi
11.(7
23.33
35.00
Til* (tin)
4U7
58.33
fleeiss*^
coc \L-L-
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P715
Sample Number: 9S194
Operator :
T ime
Study
8/30/39 9:13 AM
MCFARLAND
Inter-face #
^utoSampler
Rack/Vial
5
None
0/0
Channel
attached
A/D mV Range
1000
Data Acquisition Timet 8/30/89 3:52 AM
Delay Time
End Time
Sampling Rate
3aw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5037. raw
C:\2700\GC5\MCF5037A.rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C: \2700\GC5\MCF51B.smp
C: \2700\GCS\MCFS4B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject : 0.00
Area Threshold : 100
Multiplier : 0.67
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions
Capillary (3C -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Rat io
T smperature
Injection Tamp
Detector 1
Detector 2
Notes
VARIAN 3400 - S"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
13
= 1
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 68
Ret Time
Cm in 3
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount
u
Peak Area
CuV-sac]
Peak Ht
CuV:
Raw Amoun t
uq\L
l'0. 21 (V-BHG
12. lu D DIIC
D-BHG
1. 40
0. <\2
a 00
602.75
--703rt-4-
i ¦ ^
74.34-
-1-4-71 14-
occlb*
2.00
0. '15
0. Q'J
2iXJtt-
6LDRIN —
n r*i_n aakic
14.95
^>271,50
2Q37.10
22,31
SI. 02
fi 'GHLDANE
0. 4 4
77-T An
17" • i
—isx^as
0. 64
-------
¦w£
=4-Bt
¦££-
-"-i
967130.25
Q16191OQ
325.66
DDt>
1 L
00
'1') h T
CMnnci ii catc
g 1 i
EHDKETD
A-y
' • fc w
61. 40
DBC
247.
02
279087.00
24029.09
368.69
i s
Total Area = 1391773.73
Total Concentration = 505.9161
Report by Doherty Bresnahan
Q60t57TPfi
cCulOk
-------
FileNaw : C:\2700\6C5\flCF3037.ran Date: 8/30/89 9:14 AH Paqe 1 of 1
Start Tiu< 0.00 ain End Tiae> 70.00 ain Low Point: S249 uV High Point: 806661 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mV Plot Scale: 100 aV
Chrctatogra*
I
II
i
9 W 3 «£ S?,?S3 CSfiS SSXStf *63ft*3 bite
2 «J5 J! tZ B RS ERaA X KMH9 C5!! SB P D tin I » 1 Ift
ra
JL±*L
H •
a t - 5 .
V * 3 s , 3
a *
i i
* i T
nw 23.33 35.00 #.w
Tiw («in)
i1 ¦
58.33
«OOt5«-u.3
C&G
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
tPA SAMPLE MO.
P803
Lab Names LOCKHEED-ESC
Contract: 68-03-3249
Lab Code: Case No. :
Matrix: (soil/water) SOIL
Sample wt/voi: 30 grams
Level: (low/med) LOW
*/. Moisture: not dec. 1.7 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.: —— SDG No.:
Lab Sample IDs 9S179
Lab File ID:
Date Received: 7-25-89
Date Extracted: 7-31-89
SONC Date Analysed:
Dilution Factor: 10
CONCENTRATION UNITS:
ug/kg 0
319-34-6 a lpha-BHC
319-85-7 beta-BHC
319-86—3 del ta-BHC
53-89-9 gamma-BHC (Lindane)
76-44-8 Heptach lor
309-00-2 A1 dr in
1024-57-3 Heptachlor epo:;ide
939-98-8 Endosu 1 -fan I
60-57-1 Dieldr in
72-55-9 4, 4' -DDE
72-20-8 Endrin
33213-65-9 Endosul-fan II
72-54-8 4,4'-DDD
1031-07-8 Endosu 1 -fan sul tate
72-43—3 Mstho;
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P803
Sample Number: 9S179
Operator
Time
Study
8/30/89 1:49 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89 6:50 AM
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File : e:\pkd\MCFR025.raw
Result File : e:\pkd\MCFR025.rst
Instrument File: e:\pkd\pkd.ins
Process File : e:\pkd\pextstd.prc
Sample File : e:\pkd\clpa.smp
Sequence File : e:\pkd\MCFRLND.seq
Inj. Volume
Sample Amount
2 uL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT1*
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Rat Tlaa
[min)
Covenant
Adjuatad Afflounc Raw Amount Paak Araa Paak Bt
US/L UG/L [uV-sac] tuV)
MULTIPLIER
Adj/IUw
%
i ts r.mr
IIBPEPWi
9it» BtBBI
19.89 PIKgaiM
;3. 39
17.68 OPT
H.88 BIIBMJ
23.61 OBC
B.li
i.18 maB.aa
-8.88
r&i-
a.it laam.aa sos9iit
ia.*i
0*i70
u.m »
114.17
~rW
16$. 20
2.24a6 31443.41
a.aa
0.60-
9.66
o.ao
a. ta
8.48
0.68
Total Araa • 8571060.00
Total Concanczatlon ¦ 440.4071
Report by Tim Rand, Lockheed-ESC
aaaaea:
C cO i'^ '
-------
Chroma tioararo
FileNaae : e:\pfcd\HCFR02S.rau Date: 8/30/89 1:49 PH Page 1 of 1 ^
Start Tine: 0.00 ain End Tina: 47.00 ain Low Point: -172SS77 uV High Point: 1959030 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mi Plot Scale: 250 mV
ad
250.000
208.333
125.000
333
PT
-0.000
7.83 IS.67 23.50 31.33 39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P803 Time : 8/30/89 2:29 PM
Sample Number: 9S179 Study : MCFARLAND
operator :
Interface #
AutoSampler
Rack/vial
2 Channel : 8 A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
6:50 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume ;
Sample Amount ;
e:\pkd\MCFR025.raw
e:\pkd\MCFR025A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
* * * * * EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
sassnsssssss
R«C flSM
Caia]
CoflpocttsM*
Mjuatad Mmnt IUw Amount Nik Art* t*ak He MULTIPLIER
UG It 0C/L (uv; Adj/Raw
a o Ci.cai.Mm
11 19 t.ffBLBOiiHI
10 »3 ppg
11 oi Eimatit
¦>l »a BBB
ti.io mnwowjoM
23.61 DSC
rW-
i8.li eg woo. oo ijea?9i
?W"
!.«.b» inaiB.aa lmn.asi
-nr
—»T
w
ua.u
0"'p8»
z.snv
10T330.W
—aaa.a* ¦
19.81 HUJBB.lt
59.O |]»>g0i0»
/BSB.it
isori. o-9
136.63
200.94
2.24*6 31463.41
flrM \'f-
vrss
~9
rsv
it-
-it.
0.6S
Total Ar«m ¦ 6401040.00
Total Concentration - 301.8*11
Report by Tim Rand, Lockheed-ESC
sasssssaasss
iCO I'13
-------
Chromatoqram
FileMaae : e:\pkd\MCFR025.raw Date: 8/30/89 2:29 PH Page 1 of 1 ^
Start fiae: 0.00 ain End fiae: 47.00 afn Low Point: -1725577 uV High Point: 1959030 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 uV Plot Scale: 250 raw
250.000
208.333
166.667
12S.00Q
-C
n,
-0.000
7.83 15.67 23.50 31.33 39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P803
Sample Number: 9S179
Operator :
T ime
Study
8/29/89 1:15 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time:
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount :
Noise Thresholds
Dilution Factor:
Divisor :
0.00
70. 00
1.0
8/29/89
min.
min.
pts/sec
11:20 AM
C:\2700\GC3\MCF5023.raw
C:\2700\GC5\MCF5023.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject : 0.00
Area Threshold : 100
Multiplier : 0.68
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capi1lary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Rat i o
T emperature
In j ec t i on Tamp.
Detector 1
Detector 2
Notes
VARIAN 3400 -5"
.25MM ID .25UMFILM RTX3
30M
HE
20CM/SEC LINEAR VELOCITY
15 PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 87
Ret Timt
[min ]
*********
Component
Name
EXTERNAL STANDARD REPORT *********
Adjusted Amount Peak Area Peak Ht
uq\L CuV-sec] CuV]
Raw Amount
ug\L
10.23 HPTCIiLr<
¦21.36 ALDHIM
-43-
1235.50
9526« 67
914 55
¦>59. 40
r64—
1.99
¦26.20 HEPEP0X
:.00 CND01
1.93 DICLDniN
-2-.+e-
9000.50
6.60 25096.50
6.20 12966¦3fl
563.44
1955. 14
3. 20
9.02-
347. 93
¦30.22 CNDQ2
jQjQOlb'l ^
c-00 Us
.•} . 40 1 4015. 00
994.56
u . 47—ztf,
-------
'11 . Zu
CHDALD
10 ¦ 66 lfl7Wi00
...... . i^gi9flR ni
1323.62
1 Qrt r\&.
-------
rileNaat : C:\2700\GC3\HCF3023.raii Data) 8/29/69 1:13 PH Paqe 1 of 1
Start Tiiwi 0.00 sin End Tiaa» 70.00 ain Lon Paint: 5148 uV High Paint: U4Z77 uV
Vertical Scale Factor: 0.00 Plat Offwt: 0 «V Plat Scale: 100 aV
ChroiatograB
¥
UMH
ttBH
« *8 3 sgssi ;nx»
k& xs ft a»»* mnucsss ssanxncdiia hi as
NiaitiaN • i
Trfit'rrj'i'i linn!
i Illllil s
.'I i i ¦ ¦ .^i ¦ i f. i i r. i ?¦ i .t. r. ¦ i iai
58,3
1LW 23.33 35.00
Til* (mis)
fleeted
C CC ' r *
-------
Nelson Analytical 2700 Chromatography System Report Header
is=sa3=a3=3aBa33=aaaaassa=3=B==sssssa3aa==3aass=aaassBaaaaaaassssaa=s
Sample Name : P803
Sample Number: 9S179
Operator :
Time
Studv
8/29/89 2:25 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range s 1000
Data Acquisition Times 8/29/89 11:20 AM
Delay Time
Enc Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
In.i. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
m in.
min.
pts/sec
C:\2700\GC5\MCF5023. raw
C:\2700\GC5\MCF5023A. rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Re.iect : 0.00
Area Threshold : 100
Multiplier : 0.68
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
•3ol it Ratio
T smseraturs
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400 S
.25MM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
15 PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 87
Ret Time
C m i n ]
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area Peak Ht Raw Amount
ug\L CuV-secJ CuV3 ug'\L
11.63 B-BHG
¦4^ 4
;, nz
1523.33
90 .04
21.36 ALDI"
Ceo1''*
-------
¦10.35 DPP 9.Z7—11599. 50 iflqT.afl 17.73 f
4 4 >65 GNDOCULFATE : 7-r-64 20552* 3-3 14604 55 11 j 19
¦51.09 CNDKCTO H-56 1912.40 125.01 1.05-.
61.43 DBC 319.12 353240.28 24493.72 469.30
Total Area = 980982.38
Total Concentration = 469.9491
Report by Doherty Bresnahan
eeettrSTw
CCO'^'
-------
FilaNaaa : C:\2700\GO\MCF3023.raM Data* 8/29/89 2:2& PN Paga 1 oi 1
Start Tiaat 0.00 tin End Tia»« 70.00 ain Low Point) 5148 uV High Point: 114277 uV
Vortical Seals Factor: 0.00 Plot Offset: 0 oV Plot Scale' 100 aV
Chrcmatograi
1MH
ttja—
5 5»«H
; RS 3 5 W I?** S«P*S*SW *3* 5?
- ! J SB XXK ass* «hk:9595 9;aft*H*R8S SSI II
.s»4 '
•'r hi ii i,i—iiiiii nirinirenn
[
sin
- u -
3 5 5-!
i 4JLJL1
I
. |
5 , r
a
1
~3U
1167 23.33 35.00 «.(7 S9.33
Tilt (ain)
000169- ¦90.
CCO I to
-------
80
PESTICIDE EVALUATION STANDARDS SUMMARY
tab Kane: ~/z Contract:-.^'C 7 - Z299
Lab Coda:
Case No.:
~7
SAS No.
SDG No.:
Instrument ID: 'mJ&GG 'l* GC Coluffl* 27^0/2V0/ Pirn
Dates o£ Analyses: *£/to ^7"?£
Evaluation Check for Linearity
PESTICIDE'
Aldrin_
Endrin"
4,4'-DDT
DBC
| CALIBRATION
| FACTOR
| EVAL MIX A
; | aanaasnan:
I///*? TCP -
7/9 7fg»g
10.0% RSD, plot a standard curve and determine the ng
for each sample in that set from the curve.
Evaluation Check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)
INITIAL
oil
EVAL
MIX
B
02 |
EVAL
MIX
B
03 |
EVAL
MIX
B
04 1
EVAL
MIX
B
05 |
EVAL
MIX
B
06 |
EVAL
MIX
B
07 |
EVAL
MIX
B
08 |
EVAL
MIX
B
09 |
EVAL
MIX
B
101
EVAL
MIX
B
HI
EVAL
MIX
B
121
EVAL
MIX
B
13 |
EVAL
MIX
B
14 1
EVAL
MIX
B
DATE
ANALYZED
-------
3D
PESTICIDE EVALUATION STANDARDS SUMMARY
Lab Names LOCKHEED-ESC Contracts 63-03-3249
Lab Code: Case No.: SDG No.:
Instrument IDs VARIAN 3400 GC Column IDs FSCCRTX5
Dates o-f Analyses 3—28-09 to 0-30-89
Evaluation Check •for Linearity
! ! CALIBRATION! CALIBRATION! CALIBRATION! */.RSD !
I PESTICIDE ! FACTOR ! FACTOR ! FACTOR ( I-f > 10.0'/. RSD? plot a standard curve and determine the ng
tor each sample in that set from the curve.
Evaluation Check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)
«
1
DATE
TIME
ENDRIN
4,4'-DDT
COMBINED
1
ANALYZED
ANALYZED
(2)
Jsaaassasasas
=sssas3ssss=
S = S33SSS33Sa
3SH33SS3SSS
========
=========
! INITIAL
3/28/89
0923
5.8
4.6
01! EVAL MIX B
8/29/89
0831
6.5
7 1
• »
02! EVAL MIX B
r*»— 1
8/30/89
0054
3. 1
4.7
1 i
04 !
05!
06 !
07!
OS!
09!
10!
¦
11 !
12!
13!
14!
1
l
(2) See Form instructions.
FORM VIII PEST-1
000182
-------
30
PESTICIDE EVALUATION STANDARDS SUMMARY
Lab Nana: Znc.£/\tr/ -/fZCL Contract
Lab Coda:
Case No.:
—7
SAS No.:
SDG No.:
Instrument ID: >//? 1 9nr, -dr
Dates of Analyses: *%/to
GC Column ID: 2^0/aVQ/jP^n
L/k?
Evaluation Check for Linearity
PESTICIDE
Aldrin
Endrin
4,4'-DDT
DBC "
| CALIBRATION
| FACTOR
| EVAL MIX A
7 yy -rc-cc
7/9 -rccc
000
~>t £ COCO
Z A
4/C C/
/A~9
/ 7 10.0* RSD, plot a standard curve and determine the ng
for each sample in that set from the curve.
(1)
Evaluation check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)
tmm
INITIAL
Oil
EVAL
MIX
B
02 |
EVAL
MIX
B
03 |
EVAL
MIX
B
04 |
EVAL
MIX
B
05 |
EVAL
MIX
B
061
EVAL
MIX
B
07 |
EVAL
MIX
B
08 |
EVAL
MIX
B
09 |
EVAL
MIX
B
10 |
EVAL
MIX
B
HI
EVAL
MIX
B
12|
EVAL
MIX
B
13 |
EVAL
MIX
B
14 |
EVAL
MIX
B
DATE
ANALYZED
^M9A9
r/fc/^9
v
TIME
ANALYZED
ENDRIN
C
T~
Ll
(2) See Form instructions.
ooc \%
4,4'-DDT
J5LL
ZJL
~K7>6
COMBINED
(2)
FORM VIII PEST-1
8/87 Rev.
-------
3D
PESTICIDE EVALUATION STANDARDS SUMMARY
Lab Name! LOCKHEED-ESC Contract! 68-03-3249
Lab Cade: Case No.: SDG No. :
Instrument ID: VARIAN 3400 GC Column IDs FSCCRTX5
- f
Dates of Analyse:8-28-89 to 8-30-89
Evaluation Check for Linearity
CALIBRATION!CALIBRAT ION!CALIBRAT ION
V.RSD
PESTICIDE
FACTOR
: FACTOR
FACTOR
< 10.OX RSO. plot a standard curve and determine ':r,a rvq
for eacn sample in that set from the curve.
Evaluation Check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)
DATE
TIME
ENDRIN
4,4'-DDT
COMBINED
ANALYZED
ANALYZED
(2)
============
===========
=s==aas«saaa
INITIAL
8/23/89
0923
5.8
4. 6
01
EVAL MIX B
8/29/89
0851
6.5
02
EVAL MIX B
3/30/89
0054
S. 1
4. 7
. j
04
05
06
07
08
09
¦
10
11
12
13
14
(2) See Form instructions.
FORM VIII PEST-I
000182
-------
8E
PESTICIDE EVALUATION STANDARDS SUMMARY
Evaluation of Retention Time Shift tor Dibutvlchlorendate
Lab Name: Lockheed-ESC Contract: 68-03-3249
Lab Code: CASE *: SDG No.:
Instrument IDs Varian 3400- ' GC Column ID: 2250/2401PK.D
Dates of Analyses: 3/29/89 TO 8/3|/89
: epa
: LAB SAMPLE
! DATE
1 TIME
i */.
i SAMPLE no.
! ID
! ANALYZED
1 ANALYZED
1 D
!============
j ============
| = = = 53 = = = ===
|===s=====a
1 =====
01:EVALA
!EVALA
18/29/89
1 1427
1 0.00
02:EVALB
:EVALB
18/29/89
1 1519
10.51
03!EVALC
:EVALC
13/29/89
1 1610
10. 12
04!INDA
i INDA
18/29/89
1 1702
1 0. 4o
05!INDB
i I NDB
!8/29/89
11754
10.31
06!TOXAPH
! TOX
18/29/89
1 1846
1 0.09
07!AR1660
!PCB1660
!3/29/89
1 1937
: o. 31
081AR1221
!PCB1221
!8/29/39
1 2029
10.31
0?!AR1232
!PCB1232
!3/29/89
1 2120
: o. 47
101AR1242
!PCB1242
13/29/89
1 ^ 4 ^
1 1 ~
1 0. 23
111AR1248
:PCB1248
!8/29/89
1 2303
10.53
12!AR1234
! PCB1254
:a/29/89
1 2356
1 0. 04
13!PBLK-1
!9S187RB
18/30/89
1 004y
10.35
14!PBLK-2
19S197RB
18/30/39
10139
10.27
15!0F01MS
!9S185MS
18/30/89
1 0230
1 0. 23
15 0F01DS
!9S186DS
18/30/89
1 0323
10.31
16!0F01
!9S177
18/30/89
1 0414
1 0. 23
17!EVALB
!EVALB
18/30/89
1 0506
10.39
13!0802
!9S178
18/30/89
1 0558
1 0. 12
I?!P303
!9S179
13/30/39
1 0650
1 0. 23
20!F1204
!?S180
13/30/39
1 0741
I O . 1 ^
21111205
!9S131
13/30/39
1 0833
l 0. 51
221M4A06
!9S132
13/30/89
1 0924
10,51
231INDA
i 100/'200A
18/30/89
1 1015
10.12
24!L4A07
!9S183
18/30/89
1 1212
10.16
25!M14A08
!9S184
18/30/39
1 1303
1 0. 19
26!H709
!9S188
13/30/89
1 1355
10
27!M510
!9S189
18/30/89
1 1446
1 0. 47
23!K411
i 9S190
18/30/89
1 1537
10. 19
29:EVALB
i EVALB
18/30/89
1 tltlS
1 f
301J212
19S191
18/30/89
1 1720
1 0.04
31:L513
19S192
18/30/89
1 1312
1 0. 08
32!D414
!9S193
18/30/89
1 1903
1 0. 04
33!P715
!9S194
18/30/89
1 1955
10.54
341 N116
!9S195
18/30/89
1 2046
! 0. 51
35!INDB
!100/200B
18/3(*/89
1 L-'l. | -5"
! o *
36!INDA
1100/200A
i
: oc
i o.crt
1
V / •
l
l
«
<
!
33:
1
1
l
1
t
i
* Values outsi
0.3% for cap
page 1 of 1
de of GC limits
illary columns)
FORM VIII PEST-2
(2.07. for packed columnsi
1/87 Rev
000183
-------
8E
PESTICIDE EVALUATION STANDARDS SUMMARY
Evaluation of Retention Time Shift -for Dibutvlchlorendate
Lab Names Lockheed-ESC Contracts 68-03-3249
Lab Codes Case No.: SDG No.s
Instrument IDs Varian 340&
34!0414
!9S193
13/30/89
0437
! 0.08
35!P715
I9S194
!3/30/89
0352
! 0. 11
36!N116
I9S195
!8/30/89
0706
10. 11
37!INDB
!100/200B
!8/30/89
.rQit
! 0. 24
38!INDA
!100/200A
18/31/89
0106
! 0.23
* Values outside of QC limits (2.0% -for packed columnsi
0.3"'. for capillary columns)
page 1 of 1 FORM VIII PESTq|jQ1Q4 1/87 Rev
-------
PESTICIDE/PCB STANDARDS SUMMARY
I
ab Name:,
Lab Code:
LOCKHEED-ESC
Case No.:
I
Contract:68-03-3249
SAS No.:
SDG No.:
nstrument ID; VARIAN 3400-t
GC Column ID: /3 9ZV pfCQ
DATE(S) OF FROM:
ANALYSIS TO:
TIME(S) OF FROM: 1*Q 2.
ANALYSIS TO: 227b
DATE OF ANALYSIS
TIME OF ANALYSIS
EPA SAMPLE NO.
(STANDARD)
COMPOUND
RT
F
WIN
FROM
IT
rDow
TO
2.79
CALIBRATION
FACTOR
RT
CALIBRATION
FACTOR
QNT
Y/N
%D
alpha-BHC
beta-BHC
2.76
2.73
14900000
4.07
4.03
4.11
4500645
delta-BHC
4.72
4.67
4.77
10600000
aamma-BHC
3.52
3 .48
3.56
11700000
Heptachlor
Aldrin
4.33
4.29
4.37
10850000
5.21
5.16
5.26
12400000
Hept. epoxide
Endosulfan l—
Dieldrin
7.69
7.61
7.77
10150000
9.44
9.35
9.53
9600000
11.27
11.16
11.38
10800000
1 4.4'-DDE
10.85
10.74
10.96
9975000
1Endrin
13.22
13.09
13.35
6950000
Endosulfan II
4.4#-DDD
15.47
15.32
15.62
14025000
15.29
15.14
15.44
7725000
Endo. sufate
4.4'-DDT
21.40
21.19
21.61
4500000
17.67
17.49
17.85
4275000
Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane_
Toxaphene
Aroclor-1016_
Aroclor-1221_
Aroclor-1232~
Aroclor-l242_
Aroclor-l248_
Aroclor-l254_
Aroclor-1260_
27.21
26.94
27.48
2635000
25.77
25.51
26.03
8025000
9.19
9.10
9.28
10500000
8.47
8.39
8.55
10350000
18.07
17.89
18.25
374762
4.3
4.26
4.34
322340
2.55
2.52
2.58
195860
4.3
4.26
4.34
153150
4.3
4.26
4.34
181334
5.44
5.39
5.49
299659
13.05
12 . 92
13.18
660939
21.08
20.87
21.29
716135
1
I
I
:.on was performed, N if not performed.
Under QNT Y/N: enter Y if quantitat
1;D must be less than or equal to 15.0% for quantitation, and less than
>r equal to 20.0% for confirmation.
fote: Determining that no compounds were found above the CRQL is a form of
[piant itation, and therefore at least one column must meet the 15.0% criteria.
For multicomponet analytes, the single largest peak that is characteristic
ff the componet should be used to establish retention time and %D.
dentification of such analytes is based primarily on pattern recognition.
page j__ of
FORM IX PEST Q0018s •/« Re
-------
9
PESTICIDE/PCB STANDARDS SUMMARY
Lab Name: LOCKHEED-ESC Contract: 68-03-3249
Lab Code: Case No.: SAS No.: SDG No.:
Instrument ID: VARIAN 3400 - J GC Column ID: 2250/2401PKD
DATE (S) OF FROM: 8/Q9 fA<*
ANALYSIS TO: R/J9/753
TIMEfS) OF FROM:
ANALYS IS TO: 23
DATE OF ANALYSIS 8/3 0/8y
TIME OF ANALYSIS 1015
EPA SAMPLE NO.
(STANDARD) INDA
COMPOUND
RT
2.76
F
WIfl
FROM
IT
mow
TO
2.79
CALIBRATION
FACTOR
RT
CALIBRATION
FACTOR
QNT
Y/N
aas
%D
saaas
alpha-BHC
beta-BHC
2.73
14900000
4.07
4 .03
4.11
4500645
delta-BHC
4.72
4.67
4.77
10600000
gamma-BHC
Heptachlor
Aldrin
3.52
3.48
3 .56
11700000
3.53
12500000
V
6.8
4.33
4.29
4.37
10850000
4.33
11800000
V
8 . 8
5.22
5.17
5.27
11550000
5.22
12250000
y
6 . 1
Hept. epoxide
Endosulfan I_
Dieldrin
7.69
7.61
7 .77
10150000
7 .68
10800000
V
6 . 4
9.44
9.35
9.53
9600000
9.43
10200000
y
6. 2
11.27
11.16
11.38
10800000
11.is
11500000
y
6. D
4.4'-DDE
10.85
10.74
10.96
9975000
/
i
Endrin
13.22
13.09
13.35
6950000
Endosulfan II
4.4'-ODD
15.47
15.32
15.62
14025000
15.42
15050000
7 . 3
15.29
15.14
15.44
7725000
Endo. sufate
4.4'-DDT
21.40
21.19
21.61
4500000
17.67
17.49
17.85
4275000
17.61
4525000
5. 8
Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane_
Toxaphene
Aroclor-10l6_
Aroclor-l221~
Aroclor-l232_
Aroclor-1242~
Aroclor-1248~
Aroclor-1254_
Aroclor-1260~
27.21
26.94
27.48
2635000
27.05
2700000
2.5
25.77
25.51
26.03
8025000
9.19
9.10
9 .28
10500000
8.47
8.39
8.55
10350000
18.07
17.89
18.25
374762
4.3
4 .26
4.34
322340
2.55
2.52
2.58
195860
4.3
4.26
4.34
153150
4.3
4.26
4.34
181334
5.44
5.39
5.49
299659
13.05
12.92
13.18
660939
21.08
20.87
21.29
716135
Under QNT Y/N: enter Y if quantitation was performed, N if not performed.
%D must be less than or equal to 15.0% for quantitation, and less than
or equal to 20.0% for confirmation.
Note: Determining that no compounds were found above the CRQL is a form of
quantitation, and therefore at least one column must meet the 15.0% criteria.
For multicomponet analytes, the single largest peak that is characteristic
of the componet should be used to establish retention time and %D.
Identification of such analytes is based primarily on pattern recognition.
page <2. of
FORM IX PEST 000186 a/87 Re
-------
PESTICIDE/PCB STANDARDS SUMMARY
Lab Name:,
Lab Code:
LOCKHEED-ESC
Contract:68-03-3249
Case No.:
SAS No.:
SDG No.:
Instrument IP; VARIAN 3400-1
GC Column ID: 2250/24Q1FKD
COMPOUND
alpha-BHC_
beta-BHC
delta-BHC
gamma-BHC
Heptachlor
Aldrin
Hept. epoxide
Endosulfan I_
Dieldrin ~
4,4'-DDI
Endrin
Endosulfan II
4,4'-DDD
Endo. sufate
4,4' -DDT
Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane__
Tox'aphene ~
Aroclor-1016_
Aroclor-1221_
Aroclor-1232_
Aroclor-1242~
Aroclor-1248_
Aroclor-1254~*
Aroclor-l260~
DATE(S) OF FROM
ANALYSIS TO
TIME(S) OF FROM:
ANALYSIS TO:
« /la)9 (£9
ZHStp
RT
2.76
4.07
4.72
3.52
4.33
5.21
7.69
9.44
11.27
10.85
13.22
15.47
15.29
21.40
17.67
27.21
25.77
9.19
8.47
18.07
4.3
2.55
4.3
4.3
5.44
13.05
21.08
RT
WINDOW
FROM TO
2.73
4.03
4.67
3.48
4.29
5.16
7.61
9.35
11.16
10.74
13.09
15. 32
15.14
21.19
17.49
26.94
25.51
9.10
8.39
17.89
4.26
2.52
4.26
4.26
5.39
12.92
20.87
2.79
4.11
4.77
3.56
4,37
5.26
7.77
9.53
11.38
10.96
13.35
15.62
15.44
21.61
17.85
27.48
26.03
9.28
8.55
18.25
4.34
2 * 58
4.34
4.34
5.49
13.13
21«29
Under QNT Y/N: enter Y if quantitat
CALIBRATION
FACTOR
14900000
4500645
10600000
11700000
DATE OF ANALYSIS 8/31/89
TIME OF ANALYSIS 00T5
EPA SAMPLE NO.
{STANDARD) IND8
RT
2.77
4.08
4.74
10850000
12400000
10150000
9600000
10800000
9975000
6950000
14025000
7725000
4500000
4275000
2635000
8025000
10500000
10350000
374762
322340
195860
153150
181334
299659
660939
716135
5.23
10.87
13.23
15.33
21.43
25.76
9.21
8.49
CALIBRATION
FACTOR
17300000
5100000
12400000
13700000
11000000
7050000
8900000
4975000
7350000
11400000
11450000
QNT
Y/N
sssa
JL
T^—'
V
31
%D
16.1
13.3
trra
IZI
£
z
z
;.on was performed, N if not per
10.5
10.3
T7
1076
8.4
8.6
10.6
ormed.
%D must be less than or equal to 15.0% for quantitation, and less than
or equal to 20.0* for confirmation.
Note: Determining that no compounds were found above the CRQL is a form of
quantitation, and therefore at least one column must meet the 15.0% criteria.
For multicomponet analytes, the single largest peak that is characteristic
of the componet should be used to establish retention time and %D.
Identification of such analytes is based primarily on pattern recognition.
page 3 of nflfVfOT „ „
FORM IX PEST UUUlO# 8/87 Re
-------
9
PESTICIDE/PCB STANDARDS SUMMARY
Lab Name:
Lab Code:
T .QCKHEED—ESC
Case Ho.:
Contract:68-03-3249
SAS No.: SDG No.:
Instrument ID: v&rtrn 34.00-i
GC Column ID: 2250/2401PKD
DATE(S) OF
ANALYSIS
TIME(S) OF
ANALYSIS
FROM: a/ooTwr
TO: & /<0.0/&Q
FROM: /4-OZ
TO:
COMPOUND
RT
F
win
FROM
2.73
IT
(DOW
TO
2.79
CALIBRATION
FACTOR
14900000
RT
CALIBRATION
FACTOR
QNT
Y/N
%D
alpha-BHC
beta-BHC
2.76
4 .07
4.03
4.67
4.77
4500645
~
- V
V
~-Z
¦
delta-BHC
4.72
10600000
gamma-BHC
Heptachlor
Aldrin
3 . <52
3 .48
3.56
11700000
3.54
13100000
12 . 0
4.33
5.22
4.29
4.37
10850000
4.34
12450000
14.7
5.17
5.27
11550000
5.22
12250000
6.1
Hept. epoxide
Endosulfan l_
Dieldrin
7.69
7.61
7.77
10150000
7.69
10700000
5.4
9.44
9.35
9.53
9600000
9.43
10050000
4.7
11 .27
11.16
11 ¦ 38
10.96
10800000
11.29
11225000
3.9
4.4'-DDE
10.85
10.74
13.09
9975000
Endrin
13.22
13.35
6950000
£
5
Endosulfan II
4.4'-DDD
15.47
15.32
15.14
15.62
14025000
15.42
14175000
1.1
15.29
15.44
7725000
Endo. sufate
4.4'-DDT
21 .40
21 .19
21.61
4500000
17. 67
17.49
17.85
4275000
17.62
5875000
37 . 4
Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane~
Toxaohene
27.21
26.94
27.48
2635000
27.10
3125000
18. 6
25.77
9.19
25.51
9.10
26.03
8025000
9.28
10500000
8-47
8.39
8.55
10350000
7 ft. 07
17.89
18.25
374762
Aroclor-1016_
Aroclor-1221_
Aroclor-1232_
Aroclor-1242_
Aroclor-1248~
Aroclor-1254_
Aroclor-1260_
4 . 3
4.26
4 . 34
322340
2 . 55
2 . 52
2.58
195860
4 . 3
4 . 26
4.34
153150
4 . 3
4 . 26
4.34
181334
5.44
5.39
5.49
299659
1 3 . 05
12 .
-------
9
PESTICIDE/PCS STANDARDS SUMMARY
Lab Name:
i nn-'HFPn-pqr.
Con t r ac t: 60-03-3"?
49
Lab Code:
Case No.
•
¦
SAS No.!
SDS No.:
Instrument ID'_
Kjap t AN
ZMLQ-*"
GC Column
IDs _£
SrCRTX*
DATE(S) OF
FROM!
a-
-9B-Q9
DATE OF ANALYSIS !
ANALYSIS
TO*.
R-
-3A-M
TIME OF ANALYSIS s
TIME(S) OF
FROM 8
0809
EPA SAMPLE NO. !
ANALYSIS
TO!
iiia?
(STANDARD) !
»
i
i
RT
i I
i I
! COMPOUND
RT
WINDOW
CALIBRATION
RT
CALIBRATION
ONT: %D !
t
1
FROM
TO
FACTOR
FACTOR
Y/N! ;
! aleha-BHC
lO.'t
1 0. '20
10.34
231 4*9=1
i •
i >
! beta-BHC
It.**
• i
i t
!delta-BHC
14. 15
14. 13
1736730
t i
t
1aamma-BHC
12. 33
12.33
201=980
i i
i I
!Heptachlor
18. 12
18. 07
18. 17
968875
i *
4 4
1 A1dr i n
21.48
21.54
2023540
1 t
1 t
!Hept. epoxide
26. OS
26.00
26. 10
140460S
1 <
1 1
!Endosulfan I
30. 37
30.35
30.39
1 *f 1 QB'IA
1
1 1
!Dieldr in
33.83
711188
1 1
t i
'.4,4*-DDE
34.54
34.52
34.56
1484860
1 1
» »
!Endr in
36. 68
36 .as
4374SO
i *
1 1
1 Endosulfan II
38. 11
30.08
39. 14
1144315
1 1
I 1
! 4. 4-' -DDD
40.47
40. 45
40.49
529625
i i
t 4
!Endo. sufate
44.59
44.57
44.61
Q09498
1 4
1 *
;4.4'-DDT
45 _ 3?
45. 92
46.02
"T C ^ O "7 CT
/ W 'mi / W
1 1
t i
\ i1etho;;vch lor-
55.94
55.39
55. 99
9230lO
!Endrin ketone
51.22
51. 19
-"¦ner
51 •
516505
: a. Chiordan©
30.95
30.93
30.97
1697540
1
1
! q. Chlordane_
28.99
28.97
29.01
1685680
t
1
1 To;;aphene
50. 64
50.53
50.75
70977
)
1
1Aroclor-1016
19.91
19. 88
19.94
254733
t
1
!Aroclcr-1221
10.31
10.26
10.36
85181
I
I
i Aroclor-1232
13. 12
13.30
118604
1
! Aroc lot—1242
17.74
17.64
17.84
200099
f
1
1Aroclor-1248
^>"7 T/L
27.49
249761
I
1
!Aroclor-12S4_
35.3
35. 18
35.42
273546
<
1
1Aroclor-1260
57. 14
57.02
57.26
422693
1
1
i
i
*
1
Under QNT Y/Ns enter Y if quantitation was performed* N if not per formed.
%D must be less than or equal to 15.OX for quantitation, and less than
or equal to 20.0"/. for confirmation.
Notes Determining that no compounds were found above the CRQL is a form of
quantitation, and therefore at least one column must meet the 15.0" criteria.
For ntul t icomponet analytes. the single largest peak that is char actor i st ic
of the componet should be used to establish retention time and %D.
Identification of such analytes is based primarily on pattern recognition.
, 4 0(30189
page J_ of T_
FORM IX F'€ST a .'37 *e>
-------
9
PESTICIDE/PCS STANDARDS SUMMARY
Lab Names < nrmccn-ger Contract;Aa-AT-2?ag
Lab Codes Cass No. s SAS No. i _______ SDG No. s
Instrument IDs -rami -g" SC Column IDs Fgrri?TY^
DATE(S) OF FROMJ
ANALYSIS TO: o-M.ao
TIME "TJ.
CALIBRATION
FACTOR
RT
CALIBRATION
FACTOR
QNT
Y/N
7.D
beta—BHC
^ 1 3S
1 i eq! 1 •-> 1
79 "JO-TO:
¦del ta-BHC
1-1 t I \ J. T7
»?T.A7-rn
aamma-BHC
, _.a
1 "> " '• 1 ^ J."
->A 1 AQSA
1 2 ... 27
1 7 7 A37.5
/£
/-•
/
! 1 . •?
Hep tachlor
A1dri n
i a 1 2
,rs cit! is.17
a^ap.7=:
1 9. 1 S
1 AS44SC")
"M si
¦71 AR > SA
^A775AA
Hgpt. sPOKide
Endosulfan I_
D i e1dr i n
">a , as
14A4AA5
7A._ OS
1 -^srs
7111SB
72. B7
90OA1S
4. 4'-DDE
74 52 I 74 . SA
1aSdBAft
Endr in
4374SA !
Endosulfan II
4,4'-DDD
T.B. 1 1
7R.AR! 7R.14
114431 5
3fl. 12
957570
. 16*5
40. 47
40_ 45 i AC,. 49
529A25
Endo. sufate
44 . S9
44 . "57 ! 44. A 1
0AO40S
. Z
—. «b *
;4*-0DT
<15. <97
a«,.o-?! 4A.D2
?ceo
45.°-S-
—S. 92
S41745
!MgthCKVChlor —
SS. "54
55.39! W.oo
°--3aio
;Endrin ketone
5 a. Chlordane_
:-a. Chi or dan e_
! To:2! 57. 2A
422A9S
I I
1 1
Under QNT Y/Ns enter Y if quantitation was performed. N if not performed.
7.D must be less than or equal to 13.07. for quantitation, and less than
or eaual to 20.07. for confirmation.
Note! Determining that no compounds were found above the CRQL is a form of
Quantitation* and therefore at least one column must meet the 15.07. criteria.
For multicomponet analytes. the single largest peak that is characteristic
jf the componet should be used to establish retention time and "D.
Identification of such analvtes is based Patterri r®co<3nltion-
age J? of Lj^_
FORM IX PEST 3/87 Re
-------
9
PESTICIDE/PCB STANDARDS SUMMARY
_ab Name»
Lab Code:
nn-uFcn-cgp
Case No.:
Instrument IDs
Contract;
SAS No. s SDG No.:
GC Column IDs garpBTyw
COMPOUND
alPha-BHC
beta-BHCJ
delta-BHC.
qamma-BHC
Heptachlor
Aldr in
Hept. epoxide
Endosulfan I_
Dieldr in
4,4'-DDE
En dr i n
Endosulfan II
4,4'-ODD
Endo. sufats
4, 4'-ODT_
r-iethoxychlor-
Endrin ketone
a. Chlordane_
q. Chlordane_
Taxaphene
Aroclor-10l&_
Aroclor-l221_
Aroclor-1232_
Aroc loi—1242_
Aroclor-1248_
Aroclor-1254_
Aroclor-l260_
DATE(S) OF FROM:
ANALYSIS TO:
TIME(S) OF FROM!
ANALYSIS TO:
fl.-2aTB9.
-SaS%sSSL
t'iart9
i-i 1 a jT
RT
10.31
i;. 93
:a
is. i:
M A7
24-OS
•n ~7
mm2JXrnmhJBL
~R. 11
4Q. 47
44-
Afi.<97
¦^.U ¦ 95
IS. 99
I?i 91
10.51
13 "M
iliiZit? 4
27.56
35.:
57,14
RT
WINDOW
FROM ! TO
10» 54'
11. 9.5
tg.c»7
71 A?
:h. nn
10-
L6l—6B
"R.OS
40. 4S
44.57
45.
30.9:
£8.. 77
su - —
li 9 ¦
A£LJZt
12
17.64
,,,<¦/ » AW
-.•5 .IS
57.02
-04-
14. 17
-t:
IB, 17
X.
n 39
.83
-A.fla
iR >14
4Q. 49
44. At
02
,.JW.
22
LU25
70. ?7
29.01
.aa
22
17.94
10. -7 a
1 »-5C
17.94
17,**
.-5.4^
37.1b
¦iflUbwpvMUP
CALIBRATION
FACTOR
3114695
-zss:
-L
2C) 14380
-S4ae2S-
'141'
1 404605
131R^7n
7111 SB
lAflARAO
*374*«->
1 14**1'
•?9A7'
QH949P
lazzn
"mo
iiASQ;
1£97540
1685680
u.
Q977
S477!
85131
11 SAO4
£0009*1
249761
.¦7>*,w^6
422695
DATE OF ANALYSISfl-7i-i-aq
TIME OF ANALYSIS?^?
EPA SAMPLE NO.
(STANDARD) t imps
RT
lii.
II.90.
14. 04.
v4.,7R
40. 29
4^.41
il.V4
28.35
CALIBRATION:0NT
FACTOR IY/N
¦ SS33S33
;a9&oo
HZiO-
-LZSlMAO-
i4inr
.709515-
1619895
7.D
.¦ la
Under QNT Y/N: enter Y if quantitation was performed, N if not performed.
%D must be less than or equal to 13.07. for quantitation, and less than
or equal to 20.07. for confirmation.
Note: Determining that no compounds were found above the CRQL is a form of
uantitation. and therefore at least one column must meet the 15.0% criteria.
3r multicomponet analytes, the single largest peak that is characteristic
¦ the componet should be used to establish retention time and *'.D.
lentification of such analytes is based priQOttlSI pattern recognition.
iae
y>
Qi
1
FORM IX PEST
}/S7 Re
-------
9
PESTICIDE/FCB STANDARDS SUMMARY
Lab Name»_
Lab Codes
Instrument
' nr^uccn-ccr
Case No.:
Con tract:
SAS No. s SDG No. :
GC Column IDs cirrgrve:
! DATE
OF
FROM: q-?o-flo
: DATE OF ANALYSISn-^i!-R9
1 ANALYSIS
TO: -hq
! TIME OF ANALYSIS^ 1,-,^
! TIME(S)
OF
FROM:
! EPA SAMPLE NO.
! ANALYSIS
TO: nOC
! (STANDARD) Tuna
<
l
COMPOUND
a 1pha-BHC.
aeta-BHC
de I ca-BHC
! RT
RT ! WINDOW
! FROM ! TO
CALIBRATION
FACTOR
; i. X\
14. i;
M-
aamma-BHC
17
33 :
1 *¦» T"^ !
1 ~,
• ^ '
Heptach lor
—1-3-f
i3.i:>7;.
13,
-IZ:
A1dr i n
71
51 !
19!
'"I
^4 1
Hept. epoxide
;!
7 a i*i i-i!
76
1 •
Endosulfan I
'1*1
T7 ¦
TA T®! !
-9 i
D i e 1dr i n
fl? 1
79i
"T T
ss!
4.4'-DDE
TA-
«14!
T4 . !
14.
=:a :
Endr in
TA.
Afl >
ta.ab!
16.
ftfli
Endosulfan II
1 i ! t:r . on!
za.
.14:
4,4'-DDD
40.
47 '•
40.45:
4<">
49:
Endo. sufate
44.
44.^7:
44.
61 :
4.4' -DDT
4«3.
07 !
as.9?!
('(7 !
;ietho::vch lor-
ss.
94 i
¦=•>5.99!
"ifi
99:
Zndrin ketone
.22:
=11.19!
=\\
23!
a. Chlordane
y.a.9y.\
97 !
a. Chlordane
99!
?s.97:
¦-•9
01 !
Toxaphene
!W
Ml
«=:<•). Fi!\:
TiO
.73!
Aroclor-1016_
19.911
17.88!
i?
¦ 74!
Aroclor-1221
10.
~1 !
1CJ.7A!
1 <">
.36!
Aroclor-1232
71 *
1^.1?:
1*
10!
Aroclor-1242
17
74!
17.A4:
17
R4!
Aroclor-124B
17
77
49!
Aroclor-1254
?.X. 3!
is. m!
ifi
. 4?:
Aroclor-1260
S7
14:
^7.09!
f!7
.?5C>??5
1 IZ*-£JSl
ONT
v/n
/>
*/.D
JJ
— 1. 5
0.7
",8. (V
9. 9
^L.,.4
Y i f
Under ONT Y/N: enter
*/.D must be leas than or equal to 15
or equal to 20.0'/. for confirmation.
quantitation was
0'/. tor
performed. N
quant i tat ion 1
if not per
and less
forme
than
d.
Note! Determining that no compounds were + ound above the CROL is a torm of
quant i tat ion» and therefore at least one column must meet the 15.07. criteria.
For mult icomponet analytesi the single largest peak, that is character ist ic
the componet should be used to establish retention time and /CD.
o+
Identification of such analytes is based pr^
page of ^
Jn pattern recognition.
FORM IX PEST
3-^1=7 Re
-------
10
FESTICZDE/PCB IDENTIFICATION
EPA SAMPLE MO.
r
Lab Nana: 1 . Contract: (c%. 'C3 ^ |
Lab Cod#:
Caaa No.
SAS No.:
SDG No.:
GC Column ID (1): R£-0 qc Coluan ID (2): F^ZCCTCifT
Inatruaant ID (1): ^ I Inatrumant ID (2): 3>KX)*b^'
Lab Saapla ZD:
Lab Fila ID: __________ (on*Y confirnad by GC/MS)
PESTICIDE/PCB
RETENTION TIME
01 ^ ^ ' - CdO^- Coluan 1 1 c-^
02 Coluan 2 3<4. ^
RT WINDOW
OF STANDARD
From to
IC.1+ /c/i L*
3
-------
-pO-4U iC&O
&COIert'*-
-------
L<-
f
U| + h(jL~^k
QOC(c^"
-------
l^-f" blt^Jc.
u£oiciL
-------
r f ,
' ^^0 lC^O if
C'CCKi^
-------
OOCI^S"
-------
a?*0 ;^+,r^
lvl+ !sLa~JC.
OCO Ic'c'
-------
ooo^°
-------
QCO i 0 *
-------
pivc/) (_ LV^X) < I I CW4
•j?ccac 5.
-------
<0 CO -i. C ~L
-------
bLz k.
Occ'^c^
-------
—rW> .pi4U. lO&g *
b-if bLc^J<.
£C O ic ^
-------
C^X<0 i i C*v\ct-^X^
4
CGPCu
-------
"TWp^u. LO*«
Ooc^t^-
-------
OCCl°^
-------
cc-ojia
-------
Sample Name : EVALA
Sample Number:
Operator : tar
Nelson Analytical 2700 Chromatography System Report Header
7:38 AM
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
2:27 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount
e:\pkd\MCFR0 0 6.raw
e:\pkd\MCFR006.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL"
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
R«c Tlaa
Caiymm
Adjusted Amount
Rav Amount
P«ak Art*
Peak flt
MULTIPLIER
[mini
UG/L
UG/L
[uV-sac)
[uV]
Adi/Raw
3.2*
AL0RIH
0.00
0.00
232993.00
16963.2
13.2*
ENDftXH
0.00
0.00
148940.00
3147.2
13.3*
000
0.00
0.00
12290.00
367.9
17. «*
00T
0.00
0.00
73940.00
2119.3
23.69
08C
o.oo
0.00
113443.00
2696.1
Total Aria • 381610.00
Total Caoeaatratloa - 1.0000
Report by Tim Rand, Lockheed-ESC
000210
-------
FileNane : e:\pkd\HCFR006.rau Date: 8/30/89 7:38 AH Page 1 of 1
Start Tine: 0.00 ain End Tiae: 47.00 Bin Low Point: 9190 uV High Point: 327490 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 OV Plot Scale: 2S0 mV
d_»
cr>
c/i
<3->
250.000-
208.333-
166.667-
125.000-
83.333-
o
o
o
ft *1.667-
-0.000-
A
"3
vn
Ol
(D
mS
CN
¦fV rr^T
I I
te! H S
Pi i Ht
&
I I I I I l"l I I | I I IT I l*T I i
7.83 15.67
I I I
T
23 . 50
Time (min)
I I I I I | l I I l I l
31. 33
I | I I I r
39.17
I I I
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : EVALB
Sample Number:
Operator : tar
Time
Study
8/31/89 2:05 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
3:18 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR007.raw
e:\pkd\MCFR007.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Sac Tlaa Co^onaat Adjusted Aoount Raw Amount Paak Araa Peak He MULTIPLIER
[min) Naaa UG/L UG/L (uV-»ac| [uV] Adj/Raw
3.22 AURIM 0.00 0.00 1.22*6 S8332.ll
13.26 EHDRIB 0.00 0.00 696223.44 24604.63
15.36 DSD O.OO 0.00 72283.00 2133.88
17.69 DOT 0.00 0.00 297440.00 S668.89
23.82 0BC 0.00 0.00 641260.00 14232.10
Total Araa - 2928104.30
Total Concentration • 1.0000
Report by Tim Rand, Lockheed-ESC
000212
-------
Chromatoaram
FlIeNane : «:\f*d\MCF*007.r»w Date: 8/30/89 7:44 AM Page 1 of 1
Start Tlaa: 0.00 aln End Tfne: 47.00 -In Low Point: 5710 uv High Point: 223570 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 MV Plot Scale: 250 mV
250.000-
c-w to
CN to
kT> ¦£>
CO tO CTI
c^( ir» to
•—» v> r-»"
Ch
*n,
\3
Of
&
o
CO
CL>
CxL
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000
JH
Sr
t r
A
rA
C3
e»
i ii it
I I I I I I I I I I I I I I I
7 .83
fi i^iFi i Fil
&
15. 67
i i i i i i i i i n i i i i i i j i i i i i i i i i | i i i i i i i i i
23.50 31.33 39.17
Time (min)
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : IVALC
Sample Number:
Operator : tar
Time
Study
8/29/89 5:35 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/235
10000
Data Acquisition Time: 8/29/89
Delay Time : o.oo min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
4:10 PM
Raw Data File :
Result File :
instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR008.raw
e:\pkd\MCFR008.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.sap
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Rej ect
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Hat Tim Consonant Adju.e.d Anoint lUw Amount Paak Ar.» Faak Ht KULTIFtlER
'slal Haaa UO/L UG/L Jutf-«ael CuV] AdJ/ttaw
5.21 ALDSSIH
0.00
0.00
2.*3«6
181626.89
10.93 ODE
0.00
0.00
20130.00
629.33 -
11.22 EOT«H
0.00
3.30
1.41.6
*90*0.98
13.3* ODD
0.00
o.oo
318933.33
3090,07 -
17.SI DDT
0.00
o.oo
•2003*.S3
21126.99
2t.io amia
0.00
0.00
197893.86
*167.81
11.66 0BC
0.00
0.00
1.33.6
29229.83 -
fetal Araa m 6380*90.00
Total Caneaatratlea " 1.0000
Report by Tim Rand, Lockheed-ESC
000214
-------
FileMaoe : e:\pkd\MCFB008.raM
Start Tlae: 0.00 ain End Tlae: 47.00 ain
Vertical Scale Factor: 0.00 Plot Offset:
Date: 8/29/89 5:35 PH Page 1 of
Low Point: 5550 uV High Point: 265620 uV
0 bV Plot Scale: 250 mV
Chromatogram
a>
cr>
CO
a*
O
O
o
n
C/l
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
irt
5
ts
id
ro cs 75:
3 £} 3
-^n^r
^ H s
i i.i . f~j>
i i i r3? i i | i i i? i iT i i H i i i i i
to
T Is? I
7.83
V
15.67
23 . 50
Time (min)
T-r
i 'p-1! I I I I I I i i | i I i i I i i i
31.33
39.17
-------
/
5
m
a
i
r?0
C£"" {,¦
<- f C C„
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : INDA
Sample Number: 100/200A
Operator : tar
Time
Study
8/30/89 7:12 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
5:02 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR009.raw
e:\pkd\MCFR009.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
0.00
*EXTERNAL STANDARD REPORT'
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
(mini
Cacponant
Adjuatad Amount Raw Amount Paak Araa Paak He
UC/L VG/L . [uV-i«e) (uV)
MULTIPLIER
AdJ/Raw
3.32 C-BHC
100.00
100.00
2.34*6
262247
88
1.00
4.33 HPTCHLR
100.00
100.00
2.17.4
194337
48
1.00
3.22 ALOUD
100.00
100.00
2.31a6
172399
19
1.00
7.69 HEPEPOX
100.00
100.00
2.03*6
108289
73
1.00
9.44 ENDOl
100.00
100.00
1.92*6
83268
70
1.00
11.27 DIELDRIH
200.00
200.00
4.32*6
168198
41
1.00
15.47 ENDOl
200.00
200.00
3.61*6
166490
39
1.00
17.67 DOT
200.00
200.00
1.71*6
49103
94
1.00
1S.SS EHDAL8
200.00
200.00
2.62*6
33870
09
1.00
23.80 DBC
200.00
200.00
2.66*6
37072
61
1.00
27.21 MEIH0XT
1000.00
1000.00
3.27*6
120386
83
1.00
Total Araa - 3300)344.00
Total Concentration - 2500.0000
Report by Tim Rand, Lockheed-ESC
000216
-------
Chromatoqram
FileNaae : e:\pkd\MCFB009.ray Date: 8/30/89 7:13 AN Page 1 of 1
Start Km: 0.00 ain End Km: 47.00 ain Lou Point: 5310 uV High Point: 265190 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 «V Plot Scale: 250 aN
r— po o o o *—
u> Dq («-> r>< oo
l-s cd -— V yS
«— -— cn og «r-«
250.000
208.333
166.667
125.000
-0.000
7.83 15.67 23.50 31.33 39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface #
AutoSampler
Rack/Vial
INDB
100/200B
tar
Time
Study
8/30/89 7:15 AM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
5:54 PM
Raw Data File
Result File :
Instrument File:
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount
e:\pkd\MCFR010.raw
e:\pkd\MCFR010.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
kEXTERNAL STANDARD REPORT"
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Rot Tlao
Caoponant
Adjuatad Amount
Raw Amount
P*ak Ar*a
Peak Ht
MULTIPLIER
(in In)
Nana
UG11
UG 11
[uV-iacj
[uV|
Ad)/Raw
2.76
A-BBC
100.00
100.00
2.98*6
429283.2
1.00
4.07
B-BHC
100.00
100.00
900129.13
80946.6
1.00
4.72
D-BBC
100.00
100.00
2.12*6
178263.>
1.00
3.21
ALDRIN
100.00
100.00
2.48a6
181232.8
1.00
8.47
G-CHLDANI
100.00
100.00
2.07*6
101306.9
1.00
9.19
A-CSLDANX
100.00
100.00
2.10*6
92830.6
1.00
10.81
DDE
200.00
200.00
3.99*6
161777.8
1.00
11.12
esduh
200.00
200.00
2.78*6
96660.3
1.00
13.29
000
200.00
200.00
3.09*6
94)38.4
1.00
21.40
EHSOSULTAIX
200.00
200.00
1.80*6
42083.1
1.00
23.77
0BC
200.00
200.00
2.23*6
64019.4
1.00
26.22
mumu
200.00
200.00
3.21*6
70342.6
1.00
local Ar*a - 297908*2.00
Total Concentration «¦ 1800.0000
Report by Tim Randf Lockheed-ESC
000218
-------
Chromatogram
FIleNane : e:\pfcd\HCFRO10.raw Oate: 6/30/89 7:15 AM Page 1 of 1
Start Tine: 0.00 ain End Tlae: 47.00 ain Low Point: 6130 uV High Point: 434150 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 mV
Qj
CTt
CO
V iTl
CNI CN
i i*i fi i i i |'"f i 1*1* i iti r~j i
7.83 15.67
I I I I Vdl I J I I'T* I I I I l l | I I I I I I
23.50 31.33
I I | I I I I
39.17
TT
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : TOXAPH
Sample Number: TOXAPHENE
Operator : tar
Time
Study
8/30/89 12:14 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
6:46 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File
Sequence File :
Inj. Volume :
Sample Amount
e:\pkd\MCFR011.raw
e:\pkd\MCFR011.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 100.00
********** PCB/TOXAPHENE STANDARDS REPORT *****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Peak Ret Time Component Peak Area Peak Ht BL
[min] Name
[uV-sec]
[UV]
Type
1
1.53
12785.00
1.00
BB
2
2.74
4940.00
554.03
BB
3
5.68
15669.72
714.39
BV
4
6.67
25647.33
1328.33
W
5
7.77
37350.88
1293.16
VB
6
9.11
54650.00
1604.76
BB
7
11.22
151458.13
4507.26
BV
.8
12.33
125657.13
2690.70
W
9
13.04
98261.99
2786.75
W
10
13.96
32484.75
1004.78
VB
11
14.83
49962.95 •
1960.55
BV
12
15.63
225553.19
5954.49
VB
13
16.83
43039.86
1480.79
BV
14
18.07TTX
374762.56
6546.22
W
15
19.28
130638.75
2475.72
VB
16
21.19
266583.91
5837.48
BV
17
22.51
227388.50
3494.33
W
18
24.10
150732.31
3613.98
VB
19
25.71 V-C
1.21e6
26556.20
BB
Total Area = 3245562.00
=™™=«============= ==e===M====_=== QQQ22Q
-------
REPORT BY TIM RAND, LOCKHEED-ESC
000221
-------
cnromauouram
fiIcMaoe : e:\pkd\HCfR011.raw Date; 6/30/69 12:14 PH Page 1 of 1 ^
Start Tine: 0.00 ain End lias: 47.00 ain Lom Point: 4160 uV High Point: 91770 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 60 mV
*¦n
oa r— -m— cm —h-> ki oa en t— ¦—- i—
<3 r^. t- cw o do era qcs r- m r-
krt r—en — id 3 erf - pJ -*=r uS
— -— -— -— •— «— TN CM CN CM
60.000-
Oj
cr>
cry
CXl
50.000-
40.000-
30.000-
20.000-
10.000-
0.000-
H
Trf
O
o
o
ro
M
ro
i | i I I i I I I i i [ i I I i i i i i T j i i i i i i i i i j i i i i I i i i i
15.67 23.50 31.33 39.17
Time (min)
I l l I I
l | l I I I I I i I
7.83
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1660
Sample Number: PCB1660
operator : tar
Time
Study
8/30/89 12:16 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
7:37 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File ;
Sequence File :
inj. Volume :
Sample Amount ;
e:\pkd\MCFR012.raw
e:\pkd\MCFR012.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.sop
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
100.00
********** PCB/TOXAPHENE STANDARDS REPORT *********
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Peak
Ret Time
Component
Peak Area
Peak Ht
BL
#
[min]
Name
[uV-sec]
[UV]
Type
1
1.55
15640.00
1.00
BB
2
2.24
27106.38
2945.03
BV
3
2.55
123957.23
15076.48
VB
4
3.31
162595.00
17565.45
BB
5
3.85
69210.00
5408.54
BB
€
4. 20/*'6
322340.06
31442.95
BB
7
5.42
229050.00
8750.07
BB
8
6.37
17309S.45
9958.94
BV
9
6.78
162095.36
8388.17
VB
10
7.47
47090.44
2857.22
BV
11
8.13
145346.31
4522.32
W
12
8.94 >
115794.63
4892.16
VB
13
10.97
33959.34
1250.66
BV
14
11,92
330726.88
6878.43
W
15
13.01
305892.28
10403.82
W
16
14.36
657188.25
18789.72
VB
17
15.77
374447.44
10876.06
BV
18
17.31
744919.94
19933.02
W
19
18.27
587216.38
12229.08
VB
20
19.90
21970.00
880.00
BB
21
21.08 / ibe
716135.69
10977.59
BV
22
23.60
1.08e6
23242.34
VB
23
25.61 Q6
-------
25 32.82 146959.91 2116.02 BV
26 35.08 339117.00 4874.37 W
27 39.90 289010.50 919.72 VB
Total Area « 9124248.00
REPORT BY TIM RAND, LOCKHEED-ESC
000224
-------
Fileilaae : e:\pkd\HCFR012.rau Oate: 8/J0/89 12:16 PN Page 1 of 1 ^
Start Viae: 0.00 ain End liie: 47.00 ain Low Point: 5*20 uV High Point: 90250 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 tU Plot Scale: 60 mV
Qj
cr>
CO
<3_>
ct;
60.000-
50.000-
40.000-
30.000-
20.000-
10.000-
0.000-
o
o
o
t\i
N
CI
in ^GO m
""1 **2 ^
—* ix«j nS «d ^ V jri h» t7>
(«<-> r— io
»»"» V I—*
CNi DO
»»"» vr>
3
<=n
r^Tl
23 . 50
39. 17
I I I I I | I I I I I I I I I 1 I I 1 I I
7.83 15.67
-------
Nelson Analytical 2700 chromatography System Report Header
Sample Name : AXU.221
Sample Number: PCB1221
operator : tar
Time
Study
8/30/89 12:18 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2 Channel : s A/D aV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 ain.
End Time : 47.00 rain.
Sampling Rate : 1.0 pts/sec
8:29 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR0i3.raw
e:\pkd\MCFR013.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 UL
1.0000 UL
Area Reject
100.00
********** PCB/TOXAPHENE STANDARDS REPORT *********
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Peak Ret Time Component
# [min] Name
Peak Area
[uV-sec]
Peak Ht
[UV]
BL
Type
1
1.42
61265.00
10416.36
BS
2
2.24
79357.56
9621.35
BV
3
2.55/^Z./
195860.80
21713.69
VB
4
3.30
26760.00
1778.28
BB
5
4.29
13440.00
1322.15
BB
6
9.05
5165.00
205.47
BB
7
13.03
8270.00
196.78
BB
8
14.43
7985.00
264.23
BB
9
21.14
148079.75
4252.91
BB
10
24.00
149847.38
3393.39
BV
11
25.61 Qi> C
1.13e6
25666.91
VB
Total Area - 1827843.25
REPORT BY TIM RAND, LOCKHIID-ESC
:ssssas»sssas
S3 C3BKBSSSS5 SS 33S IS
SSS5SSSSSSSSSSSSSS3SSSS3
000226
-------
Chromatoqrara
filed we : e:\pkd\MCfR01J.ran Date: 8/30/B9 12:18 PH Page 1 of 1 3
Start Tiae: 0.00 ain End Tiae: 47.00 ain Lou Point: 4180 uV High Point: 11S520 uV
Vertical Scale factor: 0.00 Plot Offcet: 0 aW Plot Scale: 60 MV
60.000-
50.000-
40.000-
CL>
£5 30.000
Q
CO
20.000-
10.000-
0.000-
o
o
O
ro
ro
WW-
in
to fO
•— -*r
C^l CN CN
•j—-i-Trrr
T~r
i i i | i i i i i i i i i | i i i i
7.83 15.67
I I I | I I I I I I I I i | | i
23.50 31.33
I I I I I I
39. 17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface # :
AutoSampler ;
Rack/Vial :
AS1232
PCB1232
tar
Time
Study
8/30/89 12:20 PM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate ; 1.0 pts/sec
9:20 PM
Rav Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume .
Sample Amount ;
e:\pkd\MCFR014.raw
e:\pkd\MCFR014.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
100.00
3SSSS3SS
********** PCB/T0XAPHENE STANDARDS REPORT *********
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Peak
Ret Time
Component
Peak Area
Peak Ht
BL
#
[min]
Name
[uV-sec]
[uV]
Type
1
1.42
45250.00
6083.45
BB
2
2.23
44206.66
5809.77
BV
3"
2.55
146690.00
17316.64
VB
4
3.30
85410.00
8822.75
BB
5
3«84
33320.00
2644.87
BB
6
4.30/2*5 ~
153150.00
15077.42
BB
7
5.02
96200.00
3048.24
BB
8
6.36
79833.05
4489.99
BV
9
6.77
68784.34
3584.51
VB
10
7.47
37121.80
2279.89
BV
11
7.88
115623.84
5016.99
VB
12
9.13 >
85620.00
3548.55
BB
13
11.02
19164.17
501.15
BV
i4
11.70
18271.48
751.89
VB
15
13.05
22380.00
652.57
BB
16
15.76
13330.00
373.16
BB
17
21.14
189580.00
4703.71
BB
18
23.97
152323.50
3502.29
BV
19
25.57
1.17e6
26849.68
VB
000228
Total Area - 2579317.00
-------
REPORT BY TIM RAND, LOCKHEED-ESC
000229
-------
Chromatogram
FileNane : e:\pfcd\HCFROK.raw Oate: 8/30/89 12:20 PM Page 1 of 1 7
Start Tine: 0.00 ain End Tiae: 47.00 Bin Low Point: 10 uV High Point: 91630 uV
Vertical Scale Factor: 0.00 Plot Offaet: 0 nv Plot Scale: 60 aV
CO
£9 30.000——
20.000-
10.000-
0.000-
i
Cs< ir» co
3 3
5 S 5
CN *N
-Art A
VtT°rT
—-rr
. <<~tt
o
o
o
ro
^ri i i i i i i j i i i i i i i i i | i i i i i i i i i | i i i i
7.83 15.67 23.50
Time (min)
I
£z>
111 'pj 111111111 j 111111111
31.33
39. 17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1242
Sample Number: PCB-1242
Operator : tar
Time
Study
8/30/89 12:23 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
10:12 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR015.raw
e:\pkd\MCFR015.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e: \pkd\pkdpcb. snip
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 100.00
PCB/TOXAPHENE STANDARDS REPORT
Instrument ID: Varian 3 400-1
GC Column ID: 2250/2401
Peak Ret Time Component
# [min] Name
Peak Area
[uV-sec]
Peak Ht
[UV]
BL
Type
.... !
1.55
13090.00
1. 00
BB
2
2.55
55480.00
6985.88
BB
3
3.31
78653.30
8341.17
BV
4
3.85
49700.20
3412.91
W
5
4. 3 0 / 2* V 1
181334.84
15728.82
VB
6
5.03
97569.94
2988.31
BB
7
6.36
78035.08
4391.47
BV
8
6.78
67054.63
3652.35
VB
9
7.47
37820.00
2370.63
BV
10
7.90
120290.00
5158.90
VB
11
9.15
88970.03
3645.36
BB
12
11.02
20648.30
539.38
BV
13
11.70
18893.52
767.21
VB
14
12.97
26750.00
829.93
BB
15
15.80
21160.00
576.09
BB
16
21.15
159590.00
4373.28
BB
000231
17
24.03
146121.88
3401.10
BV
18
25.63 Q4C
1.14e6
26008.06
VB
Total
Area = 2401225.00
REPORT BY TIM RAND, LOCKHEED-ESC
-------
000232
-------
FileNane : e:\pfcd\MCFR015.raw
Start Tine: 0.00 ain End Tim: 47.00 *in
Vertical Scale Factor: 0.00 Plot Offket:
« Chroma tog ram
Oate: 8/30/89 12:23 PN Page 1 of 1
Low P.iint: 3880 uV High Point: 175600 uV
0 UV Plot Scale: 60 nV
ro u> a in
S S S3 35 s
vr"»
60.000-
• • • • •
ro h~>
u=j
CN OvI
50.000-
40.000-
30.000-
CxZ
20.000-
10.000-
0.000-
"fT^T
•rr
O
O
O
rc
u-
CJ
I I I I
I I I I I I I
I I I I I I I I I I I I I I
7.83
15. 67
23 . 50
31.33
39 . 17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1248
Sample Number: PCB-1248
Operator : tar
Time
Study
8/30/89 12:25 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
11:03 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR016.raw
e:\pkd\MCFR016.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 100.00
PCB/TOXAPHENE STANDARDS REPORT
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Peak
#
Ret Time Component
[min] Name
Peak Area
[uV-sec]
Peak Ht
[UV]
BL
Type
1
1.55
10430.00
1. 00
BB
2
3.31
72947.79
7871.89
BV
3 .
3.78
53149.39
3455.80
W
4
4.30
292405.09
25192.52
W
5
4.71
150628.38
6309.37
W
6
5.44/1VS
299659.94
14405.98
VB
7
6.37
207240.44
12273.48
BV
8
6.79
212601.31
11391.48
VB
9
7.49
143854.73
8999.11
BV
10
7.91
479442.63
19075.98
W
11
9.16
364400.50
14000.70
VB
12
11.07
117180.41
2857.69
BV
13
11.72
100902.56
3897.18
VB
14
13.07
146360.00
4591.77
BB
15
14.43
27915.00
857.86
BB
16
15.82
108120.00
3253.83
BB
17
17.47
30551.10
926.27
BV
18
21.33
163670.88
4316.37
VB
Q00234
19
24.17
181006.00
3642.78
BV
20
25.84
1.17e6
26259.75
VB
Total Area = 4333220.00
-------
REPORT BY TIM RAND, LOCKHEED-ESC
000235
-------
Filename : e:\pkd\MCFR016.rau Date: 8/30/89 12:25 PH Page 1 of 1
Start Tiae: 0.00 ain End Tiae: 47.00 ain Lou Point: 490 uV High Point: 88100 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 60 101
ii"i ^~— ' <"•>» r-^ r^> cvi r-^
£
CO
60.000
SO.000
40.000
30.000
20.000
10.000
0.000
7.83
15. 67
23.50
Time (min)
i
I l i *P| I I I I l I I l I | I I I i l I I l l
31.33
39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1254
Sample Number: PCB-1254
Operator : tar
Time
Study
8/30/89 12:27 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
2S5/2S5
10000
Data Acquisition Time: 8/29/89
Delay Time : o.oo min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
11:56 PM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR017.raw
e:\pkd\MCFR017.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 100.00
********** PCB/TOXAPH1N1 STANDARDS REPORT *********
—Tffi'SagtggS'gg'S—<11. iiiiiaaiwga»cgn'"'iisi!3aaggs*y
660939.63
19355.64
W
10
14.38
377089.09
10080.90
VB
11
15.79
408694.97
11615.29
BV
12
17.37
598106.19
15350.61
VI
13
18.35
42730.00
1240.43
IB
14
19.55
14125.00
551.21
BB
15
21.17
288032.59
5251.17
BV
16
22.52
117935.81
2805.84
W
17
23.99
246120.92
4186.82
w
18
25.68
1.15e6
26299.70
VB
19
27.83
66630.00
1560.30
BB
Total Area = 5516259.50
:ssssaas!
-------
REPORT BY TIM RAND, LOCKHEED-ESC
000238
-------
Chromatoqram
fileName : e:\pkd\MCM017.raw Date: 8/30/89 12:27 PM Page 1 of 1
Start Tine: 0.00 ain End Tine: 47.00 Bin Lou Point: 1010 uV High Point: 91930 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 60 art/
Lt-a
s
cu
cr>
co
a>
CXL
60.000-
50.000-
40.000-
30.000-
20.000-
10.000-
0.floo-
rs u-> on lt> aa av u~> pm cn ao
23 S ^ SO "3 53 23
cj »*"» -it irt cH «—
-------
Nelson Analytical 2700 chromatography System Report Header
Sample Name
Sample Number
Operator
Interface #
AutoSampler
Rack/vial
EVALB
Time
Study
8/31/89 2:12 PM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
5:06 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR02 3.raw
e:\pkd\MCFR0 2 3.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
kEXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlma Cooponant Adjuatad Amount Saw Amount Paak Araa Paak He MULTIPLIER
(mini Kama UC/L UC/L [uV-«ae| (uVl AdJ/Raw
5.20 ALDRIN 0.00 0.00 1.33a6 100196.98
10.87 DDE 0.00 0.00 10743.00 400.00
13.17 ENDRIH 0.00 0.00 783768.69 27906.37
13.31 DDD 0.00 0.00 63760.00 1769.21
17.37 DDT 0.00 0.00 *81167.38 12381.86
23.39 DBC 0.00 0.00 748818.00 16610.87
Total Araa - 14277*4.30
Total Cooeancratlon - 1.0000
Report by Tim Rand, Lockheed-ESC
000240
-------
Chromatoqram
Filettane : e:\pfcd\HCFR023.rau Date: 8/31/89 2:13 PN Page 1 of 1 ^
Start Tfae: 0.00 ain End Tiae: 47.00 ain Low Point: 3250 uV High Point: 2KJ40 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 250 mV
a>
£>~>
o
CO
o_>
o;
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
O
o
o
in
K
L-
n
I I I I I
=2L
r- in u->
mS r-^
orv <—> crv
i- o in
• » _•
•— T if»
rJUr rArrr^rr-A
I I " I I
I I I
^ H ^ s s
Is? I i*Y I P| I Pi *T
i i i i i I i ii i
7.83
15 . 67
23 . 50
I I I I | I I I I I I I I I | I I I I I I I I I
31.33 39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : INDA
Sample Number: 100/200A
Operator :
Time
Study
8/30/89 11:12 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D raV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 32.75 min.
Sampling Rate : 1.0 pts/sec
10:15 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR029.raw
e:\pkd\MCFR02 9.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0. 00
kEXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
R«C T1m
(min)
Cooponant
Adjuatad Amount Riw Aoount Peak Aria P«ak Be MULTIPLIER
UC/L UC/L (uV-a«e) [uVJ Adj/Rav
3.33
G-BHC
10S.79
106.79
2.30*6
278088.81
1.00
4.13
HPTC9LR
108.76
108.76
2.36«6
210721.09
1.00
3.22
AL0RIN
103.97
103.97
2.43*6
182082.92
1.00
7.68
HEPEPOX
106.43
106.43
2.16*6
114827.64
1.00
9. *3
EHD01
106.00
106.00
2.04*6
90476.07
1.00
11.23
DIttDRIH
212.67
212.67
4.60*6
179601.03
1.00
13. *2
END02
214.74
214.74
6.02*6
180291.41
1.00
17.41
DOT
212.77
212.77
1.81*6
33008.00
1.00
18.SI
ENDAL0
211.31
211.31
2.77*6
37361.23
1.00
23.66
DBC
206.63
206.63
2.73*6
60163.62
1.00
27.03
MEIBOCX
1026.22
1026.22
3.40*6
123239.86
1.00
Total Araa ¦ 3*909869.00
Total Concentration • 2618.3032
y
Report by Tim Rand, Lockheed-ESC
000242
-------
Chromatogram
FileNane : e:\pfcd\HCFR029.raw Date: 8/30/89 11:13 AM Page 1 of 1
Start Tine: 0.00 ain End Km: 32.75 «fn Lou Point: 3400 uV High Point: 279730 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 DV Plot Scale: 250 ntv
hO
OJ
f>0 CN
5a
250.000-
u—> oa
*—
vrt
fx od
U> IT* CN
CN
i _? _ r
T ¦/>
«N CN
Qj
CO
o_»
Ck£
208.333-
166.667-
125.000-
aj.ju-
41.667-
-0.000-
~fr—iy\V;
UUUUV1
II . M » I < I II
©
o
o
10
CJ
TT
<-> 2
i i F*! i i i *f* i i 'r 'i i i i i i i i V 'i | i *Pi l'f i i i i | • i i » " > T"i i "| i i i i i i i i "
hi
&
5.46
10.92
16. 38
21.83
27.29
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : INDA
Sample Number: 100/200A
Operator :
Time
Study
8/30/89 11:12 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 32.75 min.
Sampling Rate : 1.0 pts/sec
10:15 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR029.raw
e:\pkd\MCFR029.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
tEXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
Cooponant
Adjiucad Amount Raw Amount Peak Araa
P*ak Bt
MULTIPLIER
[mini
Nam
UC/L
UC/L
(uV-i.c)
[uV]
AdJ/Raw
3.53
C-BHC
106.79
106.79
2.50.6
278088.81
1.00
4.33
HPTCSLR
108.76
108.76
2.36*6
210721.09
1.00
5.22
AL0RIH
103.97
103.97
2.45*4
182082.92
1.00
7.68
HEPEFOX
106.43
106.43
2.16*6
114827.64
l. 00
9 .4*1
END01
106.00
106.00
2.04*6
90476.07
1.00
11.23
0IELDRIH
212.67
212.67
4.60*6
179601.01
1.00
13.42
E8D02
214.74
214.74
6.02*6
180291.41
1.00
17.61
001
212.77
212.77
1.81*6
51008.00
1.00
18.81
EH0ALD
211.11
211.11
2.77*8
37161.23
1.00
23.66
0BC
206.61
206.61
2.73*6
60163.62
1.00
27.03
METHOXY
1026.22
1026.22
5.40*6
123239.86
1.00
Total Azaa - 14909868.00
Total Concentration - 2618.1092
Report by Tim Randf Lockheed-ESC
000242
-------
Chromatogram
FileMane : e:\pkd\MCFR029.ran Date: 6/30/69 11:13 AH Page 1 of 1
Start line: 0.00 ain End liM: 32.75 sin Low Point: 3400 uV High Point; 279730 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 mV
oca
Cn ~—
~ r-S
co oa
cd
u> u-»
vT>
CN CN
TT
cr»
CN
i T^i i i n H i
21.83
5.46
10.92
16. 38
27.29
-------
Nelson Analytical 2700 Chromatography System Report Header
I
lample Name
Sample Number
operator
interface #
AutoSampler
Rack/Vial
EVALB
Time
Study
8/31/89 2:15 PM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Jata Acquisition Time: 8/30/89
Delay Time : 0.00 min.
"?nd Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
4:28 PM
Raw Data File :
lesult File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR0 3 5.raw
e:\pkd\MCFR035.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
* * * * * EXTERNAL STANDARD
REPORT*****
Instrument ID:
Varian 3400-1 GC Column
ID: 2250/2401
fl'.at Tina
[mini
Caopenanc
Adjuatad Amount Raw Amount Paak Araa Peak Ht
UG/L UC/L [uV-iael [uV]
MULTIPLIER
Adj/Rav
3.20
ALDRIN
0.00
0.00
1.46a6
109938.22
13.19
ENDRIN
0.00
0.00
811320.00
30979.37
13.33
ODD
0.00
0.00
193030.00
3033.73
17.39
DOT
0.00
0.00
320313.00
9690.92
23. «2
DBC
0.00
0.00
804673.13
18182.20
Tool Aria ¦ 1391833.30
Total Concentration ¦ 1.0000
Report by Tim Rand, Lockheed-ESC
000244
-------
FileNane : e:\pkd\HCFR035.raw Oate: 8/31/89 2:15 PM Page 1 of 1
Start Tine: 0.00 «in End liw: 47.00 ain Low Point: 4560 uV High Point: 208630 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 Plot Scale: 250 mV
u-»
"1
CxZ
250.000-
208.333-
166.667-
125.000-
83.333-
id
crt r~r~) cn
*— m lr>
•*"» m~5 r-
r
41.667-
-0.000
KT
, ,r, , ,
r
-------
Nelson Analytical 2700 Chromatography System Report Header
ample Name :
Sample Number:
Operator
interface #
AutoSampler
lack/Vial
INDB
100/200B
Time
Study
8/31/89 12:52 AM
MCFARLAND
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
oata Acquisition Time: 8/31/89
pelay Time : 0.00 min.
!nd Time : 35.03 min.
iampling Rate : 1.0 pts/sec
12:15 AM
Raw Data File :
| tesult File :
.instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR04la.raw
e:\pkd\MCFR04la.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
~~~~~EXTERNAL STANDARD REPORT*****
instrument ID:
Varian 3400-1
GC Column
ID: 2250/2401
¦t Tla* Coaponant
MJuacid Amount Raw Amount ?*ak Araa
?*ak Ht
MULTIPUHl
(mini tlaaa
US/L
US/L
[uV-s*c|
[uV]
Adj/fUv
2.77 A-BBC
116.41
116.41
3.46*6
320271.aa
1.00
<>.08 1-BHC
114.04
114.04
1.02*6
94974.12
1.00
4.74 D-BHC
116.64
116.64
2.48*6
213025.41
1.00
5.23 ALDUS
110.37
110.37
2.74*6
206376.38
I. 00
a.49 C-CHLDAHX
110.35
110.33
2.29*6
114205.22
1.00
9.21 A-C8L0A8Z
108.78
108.78
2.28*6
103783.48
1.00
10.87 DDI
220.44
220.44
4.40*6
183093.69
:.oo
13.23 rami*
203.31
203.31
2.82*6
99567.81
1.00
15.33 ODD
230.90
230.90
3.56*6
110140.44
1.00
21.43 EHDOSULTATX
221.20
221.20
1.99*6
46369.36
1 30
23.74 DBC
263.73
263.73
2.94*6
74239.28
:.oo
26.24 U1IU1IJ
188.60
188.60
3.03*6
73963.03
1.00
Total Ana - 33077338.00
jfotal Concentration ¦ 2005.1608
Report by Tim Rand, Lockheed-ESC
h
000246
-------
Response (uV)
ifrZOOO
ihihiiIiiiiiihiIhiiiiii
ill in ii in ill in 1
mw:
-3-BHC
-FLORIN
:3-CH LQANE
ict
[NORIW
tico
f
=L
: 1.09
- 2.77
: i?3
• M
• W
• 10.B7
•ii?3
• 1133
::nkmfai[
-)EC
-18.56
- 21.0
• 24.07
- 2176
27.96
-------
Nelson Analytical 2?00 Chromatography System Report Header
ample Name : INDA
sample Number: 100/200A
Operator :
Time
Study
8/31/89 12:25 PM
MCFARLAND
nterface #
AUtoSampler
jtack/Vial
: 2 channel : B a/D mV Range
: Varian 8000 without controller
: 255/255
10000
ata Acquisition Time: 8/31/89
Delay Time : 0.00 min.
*nd Time : 47,00 min.
ampling Rate : 1.0 pts/sec
8:38 AH
Raw Data File
esult File'
nstrument File
Process File
Sample File
"equence File
Inj. Volume
¦Sample Amount
e:\pkd\MCFR04 3.raw
e:\pkd\MCFR0 4 3.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
asa—juaasaas
sasssss
~EXTERNAL STANDARD REPORT*
nstrument ID: Varian 3400-1
GC Column ID: 2250/2401
1*1 IIam
(min)
CoapoaasE
AdjuJCKd Aaoixax. Staw Amount F**k An*
US/L mi [uV-««e)
P«*k Be
[uVJ
KUITXH.XER
Adj/Rsv
3.3*
4.34
S.22
7.69
9,43
11.26
13.42
17.62
18.82
as.jo
27.10
G-SBC
HPTCHT.B
AUKIH
HEPEPOX
EHD01
DlttDRIB
EHD02
DDT
OISALD
DBC
1U.89
ItS.10
106.06
105.59
10*.8*
207.8*
202.43
274.93
214.48
206.34
1186.16
111.89
113.10
108.06
103.39
104.64
207.8*
202.43
274.93
214.48
206.34
1188.16
2.62*6
2.49*6
2.43*6
2.14*6
2.01*6
4.49*6
3.67*6
2.13*6
2.81*6
2.73*6
6.23*6
307318.97
231041.13-
188993.38
117871.97
92332.76
181328.36
178634.41
69639.20
60860.88
61913.21
145803.72
.00
.00
.00
.00
00
00
00
00
00
00
00
ockl Ar«» - 16090736.00
ot*l Concmtriclon - 2833.6*33
¦toport by Tim Rand, Lockheed-ESC
000248
-------
\ „ , Chromatogram
FileNrae : e:\pkd\MCFRCK3.raw Date: 8/31/89 12:25 PH Page 1 of 1
Start Tiae: 0.00 afn End Tiae: 47.00 ain Lom Point: 9270 uV High Point: 317260 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 »V Plot Scale: 2S0 mV
-— CN (O
cri -f
io cn
CO
r-*
Q_>
cr>
CO
(L)
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
L
fnf
Tf
I
r
iii i i i
t in rv o
<->>4 CN CN CM
c
o
o
10
(X)
39. 17
23.50
lb . 67
7 .83
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
pmple Number
erator
EVALA
T ime
Study
8/28/89 10145 AM
MCFARLAND
iter-face #
;toSampler
ck/Vial
5
None
0/0
Channel
attached
A/D mV Range : 1000
ftftta Acquisition
lay Time
e" d Time
Sampling Rate
w Data File :
F~.suIt File :
instrument Files
ocess File
mp1e File
Sequence File
tj. Volume
mple Amount
Timet
0.00
70.00
1.0
8/28/89
min.
min.
pts/sec
8109 AM
C:\2700\GC3\MCF3002. raw
C:\2700\GC3\MCF3002.rst
C:\2700\GC3\F0E.ins
C!\2700\GC3\EXSTD.pre
C:\2700\GC3\MCCEVAL.smp
C:\2700\GC3\MCF34A. seq
2 uL
1.0000
Area Reject
: 0.00
^3ise Threshold:
lution Factors
visor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
1.00
0.00
Bunch Factor:
istrument Conditions:
pi liary GC -
Instrument :VARIAN
Column : .23MM
Column Length : 30M
Carrier Gas : HE
Flow Rate : 20CM/SEC
Split Ratio :
Temperature : 160
Injection Temp.: 200
Detector 1 : 300
Detector 2 :
Notes :
3400
ID .2SUMFILM RTX5
LINEAR VELOCITY 15" PS I
1/MIN TO 230
Total Number o-f Peaks Detected! 18
.»at Time
Cmin]
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L CuV-sec3
Peak Ht
CuV3
Raw Amount
ug\L
1.62
1.81
3.69
12.37
21.34 ALDRIN
30.48
000250
3783.02
44434.30
787.00
486.30
0.00
02.50
11370.03
88308.39
1374.00
973.00
43177.02
403.00
4433.36
3192.76
16.82
34.77
2963.23
31.32
5785.02
44154.30
787.00
486.50
0.00
202.30
-------
36.71 ENDRIN 0.00 10861.00
38.19 365.50 731.00
41.05 DDD 0.00 1769.00
44.09 1592.00 3184.00
46.01 DDT 0.00 15612.00
51.24 ENDKETO 0.00 604.50
54.31 633.75 1267.50
55.93 961.501923.00
60.15 318.50 -
61. o3 DBC 0. 00
64.34 682.75 1365.50
65.86 483.50 967.00
S66.29
0. 00
57.03
365.50
155.o2
0.00
270.39
1592.00
1362.35
0.00
52. 48
0.00
108.07
633.75
115.84
961.50
62.26
318.50
•944.48
0.00
113. 15
682.75
86.27
483.50
Total Area = 197462.16
Total Concentration = 56452.8164
Report by Doherty Bresnahan
000251
-------
FileNaw t C:\Z700\6C3\»CF3002.rw Oatai 8/2B/89 10t4S All Pag* 1 of 1
Start Tiatt 0.00 ain End Tiaa» 70.00 ain Lot Pointi 4927 uV High Pointi 9550 uV
Vertical Scale Factor« 0.00 Plot Offwti 0 aV Plot Scalai 100 aV
Chiaaatograi
> a
UUH
0J8-;
IShi
- * « * -
ill ; ::
* !S KS
a »B ii si
JMH
aar
HW-t
nih-
il n ii ii ii fi nci mi ii
t«
111
liw
J .
a ¦ a
* I ' '
23.0
¦ 111
3.33
3S.0I
TIm (lin)
1H.il
000252
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
EVALB
T ime
Study
8/20/89 10!47 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
O/O
A/D mV Range : lOOO
Data Acquisition Times 8/28/89 9:23 AM
De 1 ay T i me : 0. 00 m i n.
End Time : 70.00 mm.
Sampling Rate : 1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5003.raw
C:\2700\GC5\MCF5003.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCCEVAL.smp
C:\2700\GC5\MCF54A-seq
Inj. Volume
Sample Amount
2 uL
1. 0000
Area Reject
o. 00
Noise Threshold: 1
Dilution Factor: 1.00
Divisor : 1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
1.00
0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .2SUMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 14
Ret Time
Cmin D
Componen t
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L CuV-sec3
Peak Ht
CuV]
Raw Amount
ug\L
1.62
1.83
3.73
21.55 ALDRIN
24.65
34.62 DDE
1888.39
12233.56
3776.78
24467.11
9672.03
08708.50
625.50 1251.00
0.00 1134.00
000233;::»20i
1106.85
942.58
50.95
131wO.58
98.00
73.58
isse.3?
12233.56
4936.02
0. 0<
625. 5<
0. 0<
-------
36.74 ENDRIN
40.79
41. 13 DDD
46.05 DDT
48.38
51.28 ENDKETO
60.21
61.37 DBC
0.00
766.34
0.00
0.00
269.50
0.00
1458.00
0.00
50453.00
1532.69
1893.44
63466.98
539.00
3090.00
2916.00
44098.00
4049.02
76.71
137.32
5601.20
41.66
254.53
279.92
4034.73
0. 00
766.34
0.00
0.00
269.50
0.00
1458.00
0.00
1_tal Area = 417000.56
Total Concentration = 22077.3047
Bpport by Doherty Bresnahan
000254
-------
FileNaaa : C:\2700\GC5VCF3003.Ptt Date: 8/28/09 10:48 AH Page 1 of 1
Start TiM< 0.00 ain End Tine* 70.00 ain Lm Point) 4911 uV High Point: 13240 uV
Vertical Scala Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Chrciatogra*
C.JB-
m
I
A
U.W
23.33
35.00
Tiie (us)
58.33
000255
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
Inter-face #
AutoSampler
Rack/Vial
EVALC
5 Channel
None attached
0/0
Time
Study
8/28/89 11:55 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition Time« 8/28/89 10:37 AM
Delay Time : 0.00 min.
End Time : 70.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File :
Result File :
Instrument File>
Process File :
Sample File :
Sequence File
C:\2700\GC3\MCF5004.raw
C:\2700\GC5\MCFS004A.rst
C:\2700\GC3\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCCEVAL.smp
C:\2700\GC5\MCF54A.seq
Inj. Volume : 2 uL
Samp 1e Amoun t : 1.0000
Noise Threshold: 1
Dilution Factors 1.00
Divisor : 1.0000
Area Reject
Area Threshold
Mult ip1ier
Additive Constant
0.00
100
1.00
0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Spirt Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PSI
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 17
Ret Time
Cmin]
Componen t
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L CuV-sec3
*********
Peak Ht
CuV3
Raw Amount
ug\L
1.62
1.80
3.55
J1.49 ALDRIN
24. 61
54.58 DDE
5614.23
40711.41
3781.00
11228.46
81422.83
7362.00
0.00 387716.50
Q00256
1599.00
0. 00
3198.00
2258.00
4751.32
2962.49
54.98
22815.53
193.06
138.91
5614.23
40711.41
3781.00
0.00
1599.00
0.00
-------
36. 70
ENDRIN
0.00
92654.00
7056.73
0.00
40.76
1508.21
3016.42
144.35
1508.21
41.11
DDD
0.00
3266.55
245.01
0.00
46.05
DDT
0.00
121951.50
10624.09
0.00
50.66
278.00
556.00
47.33
278.00
51.29
ENDKET0
0.00
6441.00
527.38
0.00
53. 08
315.50
631.00
55. 11
315.50
56.58
315.00
629.99
52.92
315.00
60.24
2943.46
5886.92
528.54
2943.46
60.72
3820.82
7641.64
345.49
3820.82
61.40
DBC
0.00
81798.00
7558.70
0.00
Total Area = 817858.31
Total Concentration = 60886.6328
Report by Dohertv Bresnahan
000257
-------
FiltNaw : C:\2700\6C3\MCF3004.ru Datat 8/28/89 11:36 AN Pa$a 1 of 1
Start Tiae« 0.00 ain End Tiaai 70.00 ain Lom Points 4942 uV High Pointi 27922 uV
Vertical Seals Factor! 0.00 Plot Offwti 0 «V Plot Seals* 100 aV
Chroutograa
3J.M
Tilt (tin)
000258
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Numbers
Operator s
100/200 A
Time
Study
8/29/89 a:47 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
5 Channel
None attached
O/O
A/D mM Rang*
1000
Data Acquisition Timet 8/28/89
Delay Time i 0,00 min.
End Time : 70,00 min.
Sampling Rate : 1.0 pts/sec
II PM
Raw Data File
Result File
C:\2700\GC5\MCF5007. raw
C!\2700\SC5\MCF3007B. rst
Instrument File! Cs\2700\GC5\FOE.ins
Process File
Sample File
Sequence File
CJ\2700\GC5\EXSTD. pre
Cs\2700\GC5\MCF51 A. smp
Cs\2700\GC5\MCF54A. seq
In ,j. Volume
Sample Amount
2 uL
1.0000 UG/kq
Area Reject
: 0.00
Noise Thresholds 1
Dilution Factors 1.00
Divisor : 1.0000
Area Threshold '• 100
Mu 11 i p1i er : 1. 00
Additive Constants 0.00
Bunch Factors 1
Instrument Conditions!
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
In j ec t i on Temp
Detector 1
Detector 2
Notes
3400
ID .25UMFILM RTXJ
sMARIAN
s .25MM
30M
HE
20CM/SEC LINEAR VELOCITY IS
160 1/MIN TO 230
200
300
PSI
Total Number of Peaks Detected! 30
********** EXTERNAL STANDARD REPORT
Ret Time
CminJ
Component
Name
Adjusted Amount Peak Area
uq\L CuV-sec J
tftft******
Peak Ht
CuV]
Raw Amount
uq\L
1
58
G-BHC
18.12 HPTCHLR
21.47 ALDRIN
26.05 HEPEPQX
30.37 END01
33.82 DIELDRIN
000259
100.00 403396.00
100.00 193774.50
100.00 429065,00
100.00 280921.00
100.00 263714.13
200.00 284475.13
23713.33
10687.36
27670.81
19015.28
18518.12
21516.71
100.00
100.00
100.00
100.00
i 00.00
200.00
-------
38.11 END02
40.99 ENDALD
43.97 DDT
53.94 METHOXY
¦ 61•DBC
200.00 457726.00
200.00 188465.50
200.00 314350.25
1000.00 369524.00
200.00 192333.00
35802.02
14856.85
27228.23
33898.45
17875.01
200.00
200.00
200.00
1000.00
200.00
. al Area - 3377744.50
"ocal Concentration = 2500.0000
Report by Doharty Bresnahan
000260
-------
FileMiM : C:\2700\GC3\nCF5007.raM Date: 8/29/89 8:48 Ml Page I of I
Start Tine: 0.00 «in End Tiae> 70.00 ain Low Point) 4991 uV High Point: 40878 uV
Vertical Scala Factor: 0.00 Plot Offset: 0 nV Plot Seals: 100 aV
Ckrautograi
SS 33s:
si ii mm
55* ft KM
m
I
¦m
23.33
8.00
Til* (lin)
0002G1
-------
Nelson Analytical 2700 Chromatography System Report Header
nple Name :
Imp la Numberi
orator :
100/200 B
Time
Study
9/29/99 8:2:
MCFARLAND
AM
[ufcer-face #
iBtoSampler
»:k/Vial
5 Channel
Nona attached
0/0
A/0 mV Range : 1000
Data Acquisition Timet 8/28/89
I lay Time : 0.00 min.
d Time > 70.00 min.
3 npling Rate : 1.0 pts/sec
4i43 PM
4|w Data File
Vault File
I atrument File:
||ocess File
»nple File
Pquence File
C:\2700\GC3\MCF3008.raw
C:\2700\GCS\MCF3008.rst
C:\2700\GCS\F0E.ins
C:\2700\GC3\EXSTD.pre
C:\2700\GC3\MCF31B. smp
C:\2700\GC5\MCF54A.ses
1
j. Volume
nple Amount
2 uL
1.0000 UG/kg
Area Reject
: 0.00
^Joise Threshold: 1
Ilution Factor: 1.00
visor : 1.0000
Area Threshold
Mu 11 i p1i er
Additive Constant
100
1.00
0.00
Bunch Factor!
1
strument Conditions:
Pi liary GC -
Instrument JVARIAN
Column : .23MM
Column Length '• 30M
Carrier Gas J HE
Flow Rate : 20CM/SEC
Split Ratio :
Temperature : 160
I n j ec t i on T emp. : 200
Detector 1 : 300
Detector 2 :
Notes :
3400
ID .25UMFILM
RTX3
LINEAR VELOCITY 15 FSI
1/MIN TO 230
1. tal Number of Peaks Detected: 29
Ft Time
.min]
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L CuV-sec]
Peak Ht
CuV]
Raw Amount
ug\L
10.31 A-BHC
11.98 B-BHC
14.IS D-BHC
21.51 ALDRIN
28.99 G-CHLDANE
30.95 A-CHLDANE
000262
100.00 462939.00
100.00 136307.00
100.00 347346.00
100.00 404708.00
100.00 337136.16
100.00 339307.94
23814.83
8792.30
21337.44
26177.13
23012.71
23824.02
100.00
100.00
100.00
100.00
100.00
100.00
-------
34.54 DDE
36.68 ENDRIN
40.47 DDD
44.59 ENDOSULFATE
51.22 ENDKETO
61.35 DBC
200.00 593944.00
200.00 174980.00
200.00 211850.30
200.00 363798.50
200.00 206602.00
200.00 151393.00
48390.96
13736.97
17901.48
27975.96
16834.00
14051.65
200.00
200.00
200.00
200.00
200.00
200.00
Total Area = 3750711.75
Total Concentration = 1800.0000
Report by Doherty Bresnahan
000263
-------
leNut : C:\2700\GC5\nCF500e.rw Date: 8/29/89 5:22 AH Pap 1
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
TOX
T ime
Study
8/29/89 8:26 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Times 8/28/89 5s!
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
70.00
1.0
min.
min.
pts/sec
C s\2700\GC5\MCF5009.raw
C:\2700\GC5\MCF5009.rst
C:\2700\GC5 \FOE.ins
C:\2700\GC5\EXSTD.pre
C:\27G0\GC5\MC5T0X.smp'
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
1.00
0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument JVARIAN
Column : . 23MM
Column Length : 30M
Carrier Gas : HE
Flow Pate : 20CM/SEC
Sp1i t Ratio :
Temperature : 160
Injection Temp.: 200
Detector 1 : 300
Detector 2 :
Notes :
3400
ID .25UMFILM
RTX5
LINEAR VELOCITY 13 PS I
1/MIN TO 230
Total Number o-f Peaks Detected: 64
Ret Time
Cmin ]
Component
Name
EXTERNAL STANDARD REPORT ****"—
Adjusted Amount Peak Area Peak Ht
ug\L CuV-sec] CuV]
Raw Amount
ug \L
1.62
1.79
10.25
13.-01
21.23
23.49
000265
112421.69
704886.63
151.00
121.50
4211.75
522.00
224843.38
1.40e6
302.00
243.00
3423.50
1044.00
S6595.30
48579.13
33.95
23.67
461.93
44.87
112421.69
704886.63
151.00
121.50
4211.75
522.00
-------
27.
29.
30.
30.
31.
34.
34.
35.
36.
36.
37.
38.
3a.
39.
39.
40.
40.
41.
41 .
42.
42.
43.
44.
45.
45.
46.
47.
48.
48.
49.
49.
49.
50.
50.
51.
52.
52.
53.
54.
55.
55.
56.
57.
57.
58.
58.
59.
59.
60.
60.
61.
62.
62.
68.
63
86
19
27
62
95
03
39
74
54
85
20
19
71
42
08
89
61
89
55
90
53 -TeXAPHENE
86
63
11
40
•J -J
83
55
63
46
77
15
55
93
64
96
90
28
86
45
72
56
91
65
14
68
09
69
53
14
81
32
52 •
90
90
DDC P&
0002GB
2397.00
4794.00
243.44
2397.00
855.00
1710.00
168.81
855.00
998.25
1996.50
123.48
998.25
395.49
790.98
77. 42
395.49
947.94
1895.88
138.27
947.94
166.50
3 c* w .00
30.94
166.50
779.54
1559.07
137.98
779.54
3679.59
7359. 19
492.37
3679.59
2624.14
5248.28
319.13
2624.14
258.25
516.50
51.33
258.25
397.25
794.50
105.33
397.25
591.00
1182.00
118.50
591.00
3932.21
7864.42
460.90
3932.21
6290.95
12581.91
740.24
6290.95
726.50
1453.00
61.05
726.50
4267.49
8534.98
581.28
4267.49
2631.50
5263.00
305.36
2631.50
1835.66
3671.33
357.93
1835.66
6354.66
12709.33
833.17
6354.66
3670.75
7341.50
504.12
3670.75
3407.25
6814.50
379.00
3407.25
0.00
1196.97
86. 63
0.00
1394.64
2789.28
180.47
1394.64
1115.19
2230.38
160.36
1115.19
2705.64
5411.28
413.09
2705.64
2233.50
4467.00
298.63
2233.50
5461.50
10923.00
605.58
5461.50
7719.23
15438.45
1181.93
7719.23
7227.75
14455.50
909.65
7227.75
3502.50
7005.00
493.96
3502.50
1404.00
2808.00
250.67
1404. (50
974.40
1948.79
177.60
974.40
1358.93
2717.87
179.09
1358.93
990.40
1980.80
209.59
990.40
6146.45
12292.89
563.72
6146.45
5068.38
10136.75
681.94
5068.38
7895.98
15791.97
1148.69
7095.98
974.00
1948.00
181.81
974.00
5559.72
11119.44
. 651.29
5559.72
2062.29
4124.58
3-w-j .84
2062.29
891.50
1783.00
172.50
891.50
3133.00
6266.00
281.02
¦j 1 -i>o ¦ 00
5534.50
11069.00
567.98
5534.50
1772.73
3345.47
269.39
1772.73
1442.62
2885.23
196.18
1442.62
1334.76
2669.52
201.63
1334.76
403.72
807.44
59.20
403.72
3781.64
7563.28
611.18
3781.64
663.07
1326.14
116.40
663.07
908.50
1817.00
170.72
908.50
1088.16
2176.33
194.69
1088.16
837.57
1675.13
149.65
837.57
2584.49
5168.98
433.48
2584.49
1686.00
3372.00
271.80
1686.00
39529.50
77039.00
7254.71
39529.50
0. 00
704.75
57.55
0.00
144.93
289.86
31.98
144.93
146.00
292.00
23.08
146.00
Total Area
2000299.00
-------
Total Concentration = 999198.6230
Report by Doherty Bresnahan
000267
-------
I' fteaa : C:\2700\GC3\ICF5009.ru Ditas 8/29/89 8:27 AH Pag* 1 ofl
t Tiwi 0.00 tin End Tia*i 70.00 ain Low Point' S132 uV High Point' 91844 uV
lbkicil Scale Fictori 0.00 Plot Offsets 0 aV Plot Scalai 100 aV
Chxaiatograa
1MH
OSH
CU9-E
swH
is.so-3
ii
TT
3 t 3 a
K C B #;C35 C r»a BMBkllllB I
ii ii ii urn i miuTirmrmii'iTrimrrrrm'uTiifniih in
T~
SB.33
11(7
23.33
35.01
Tiu (lia)
«.<7
000268
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
PCB1660
Time
Study
9/29/89 9:30 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range i 1000
Data Acquisition Timet
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
70.00
1.0
9/2B/B9
min.
min.
pts/sec
7:14 PM
C:\2700\GCS\MCF5010.raw
C:\2700\GC5\MCF5010.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCC1660.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
s i). 00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
flu 11 i p 1 i er
Additive Constant
100
1.00
0.00
Sunch Factor! 1
Instrument Conditions:
Cap i1lary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sp1i t Rat io
T emperature
I n j ec t i on T emp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 1!
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected! 79
EXTERNAL STANDARD REPORT
Ret Time Component Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin] Name ug\L CuV-sec] CuV] ug\L
1.63 0.00 723783.75 248110.34 0.00
1.82 0.00 5.00e6 173345.42 0.00
0. 15 'J • 00 631.50 71 ¦ 0.00
9.37 UUUfcUJ 0<00 3979.31 209.76 0.00
9.96 0.00 3748.14 267.29 0.00
10.30 PCB1016 242.14 27564.72 1292.75 242.14
-------
11.60
13.27
13.93
14.59
15.64
16.08
16.27
16.91
17.81
1 Q
iDi W4
19.01
19.80
20.29
20.72
21.08
21.29
22.46
22.77
23.79
24.71
25.42
26.08
26.52
27.01
"J7 CTT
tim i • vJy
nfl
«¦» o • *.o
29.50
79
30. 13
30.51
31. 16
33. 27
33.98
34.87
37.09
37.71
38.79
40.21
40.69
41.57
42. 44
44.27
45.50
46.45
46.80
47.85
48.66
49. 13
49.88
50.52
50.89
51. 41
52.66
53.46
54. 13
54.95
en
WW * SmO
56. 14
57. 14
mOI W
\ ^
x kr-
f
5°^
0 ci ^ *
fC>°
000270
P3
452.24
483.38
4780.62
2135.36
1638.75
433.08
129.74
1233.78
1159.08
1050.42
922.77
1674.58
1327.74
2106.84
486.79
65.04
68.73
423.85
660.24
1819.83
115.55
122.63
276.09
176.46
1801.35
66.79
109.77
555.80
672.86
1326.
2141.
1262.
4313.
290.33
105.23
1009.97
6259.05
2976.75
469.51
6415.12
1032.37
892.83
231.43
4519.14
2594.07
657.15
257.90
912.91
3797.70
2131.52
1330.66
142.82
303.71
900.36
10475.52
00
29
,90
,02
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0. 00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0. 00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
-------
57.54
0. 00
7982.00
627.54
0.00
58. 16 PCD 1260 -Q&>
13.65
3015.47
255.33
13.65
58.83
0.00
4163.98
368.58
0.00
59.22
0.00
785.28
81. 18
0.00
60. 15
0.00
3221.00
307.17
0. 00
61.32
. 6687.04
73112.95
61.68
6184379^
~~ 6 lti4-.ii. V4
4596.90
61843.94
62.61-
-poc-o
0.00
1874.00
164.25
0.00
63. 19
26745.00
26745.00
2287.75
26745.00
64.02
32867.50
32867.50
2173.00
32867.50
66.39
1966.00
1966.00
175.89
1966.00
68.65
13676.00
13676.00
1081.90
13676.00
69.81
896.50
896.50
79.85
896.50
Total Area = 7265623.30
Total Concentration = 211363.6719
Report by Doherty Bresnahan
000271
-------
i C:\2700\H3\MCF3010.ran Oatai 8/29/89 8:33 AN Pag« 1 of 1
Tiaat 0.00 ain End Tiaai 70.00 ain Lot Point* 5112 uV High Point: 253Z73 uV
/a icil Seal* Factor> 0.00 Plot Offset: 0 aV Plot Scalat 100 aV
Chrautograa
sa
«
1
4t
I
|MMt-
ojjH
5WH
asH
Kje-I
:;x stiefcu* cu »n«: sss srsiiji aaaa a s ti
• It •
Hi—rnfinfti
s
a
X
lltf
T
23.33
4-t
35.00
TiM din)
44.0
58.2
000272
-------
Nelson Analytical 2700 Chromatography System Report Header
sssassaassas
Samp 1e Name :
Samp Ie Number:
Operator :
Interface # :
AutoSampler :
Rack/Vial '
PCB1221
5 Channel
None attached
0/0
T ime
Study
8/29/89 8!57 AM
MCFARLAND
A/D mV Range » 1000
Data Acquisition Timei 8/29/89
Delay Time s 0.00 min.
End Time : 70.00 min.
Sampling Rate : 1.0 pts/sec
8s28 PM
Raw Data File 5
Result File s
Instrument Files
Process File :
Sample File '•
Sequence File t
Inj. Volume '•
Sample Amount :
C:\2700\GC5\MCF5011. raw
Cs\2700\GC5\MCF50i1. rst
C:\2700\GC3\F0E. ins
C:\2700\GC5\EXSTD.pre
CS\2700\GC5\MCC1221.smp
C:\2700\GC5\MCFS4A.seq
2 uL
1.0000
uni ts
Noise Thresholds 1
Dilution Factors 1.00
Divisor : 1.0000
Area Reject s 0.00
Area Threshold : 100
Multiplier s 1.00
Additive Constants 0.00
Bunch Factors i
Instrument Conditions!
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected!
Ret Time
[min 3
1.62
1.81
5.72
7. 18
8. 13
9.36
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L C uV-sec 3
*********
Peak Ht
CuV3
Raw Amount
ug\L
389663.69 779327.38 276148.03 389663.69
000273
2408061.00
1509.25
349.00
1827.25
6982.00
4.81e6 175438.78
3018.50
698.00
3654.50
•j33.43
80. 73
er*T
748.20
*408061.00
1509.25
349.00
1827.25
6982.00
-------
I
To
I
9.94
10.31
PCB1221
12.87
13.28
14.59
16.92
17.81
18.55
19.92
20.37
21.31
27.55
o0.53
35.37
38.82
42.47
44.32
46.49
47.69
49. 17
52.69
57. 17
60. 19
61.34
DBC
A>'V, *
So
/v y iD'
c -V4
4024.13
0.00
437.28
2896.33
228.30
1982.49
722.73
374.50
4231.67
6666.38
1249.18
305.00
243.50
195.00
336.25
309.00
142.00
376.00
2378.00
233.50
180.25
355.75
1515.00
0.00
874.56
5792.66
437.00
3964.98
1443.50
749.00
2498/33
610.00
487.00
390.00
672.50
618.00
284.00
732.00
4736.00
307.00
360.49
711.50
3030.00
69733.00
602.69
1870.65
90.72
266.02
57. 13
203.81
105.43
61.27
240.14
323.26
148.46
46.59
44.91
36.90
66.44
66.95
25.62
67.77
176.30
48.01
32. 93
65.55
296.14
6456.44
4024.13
0.00
437.28
2896.33
228.50
1982.49
722.73
374.50
4251.67
6666.58
1249.18
305.00
243.50
193.00
336.23
309.00
142.00
376.00
2378.00
253.50
180.25
355.75
1515.00
0.00
tal Area = 5786695.00
Total Concentration = 2837815.0000
^port by Doherty Bresnahan
000274
-------
FileNaaa : C: \2700\GC3\MCF3011-ra* Data: 8/29/89 8:SB AH Paga 1 of 1
Start Tiaei 0.00 ain End Tiaet 70.00 ain Low Points 5113 uV High Point: 275859 uV
Vertical Scala Factort 0.00 Plot Q«s«t: 0 aV Plot Seals: 100 aV
Chroaatogra*
9 99
mm-.
m
S
a
n
«
11.(7 23.33 35.00 58.33
Tit* (ain)
000275
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
flnple Number
'P srator
I
ter-face #
toSampler
ck/Vial
PCB1232
5 Channel
None attached
0/0
Time
Study
8/29/89 9«17 AM
MCFARLAND
A/D mV Range : 1000
Ita Acquisition
lay Time
End Time
Imp ling Rate
m Data File
Result File
instrument File
¦ acess File
™mple File
Sequence File
| j. Volume
Sample Amount
Iise Threshold
lution Factor
Divisor
Timet 8/28/89 9«42 PM
0.00 min.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5012.r aw
C:\2700\GC3\MCF3012A.rst
C:\2700\GC3\F0E.ins
CJ\2700\GC5\EXSTD.pre
C:\2700\GC5\MCC1232.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
J 0.00
00
0000
Area Threshold
Multiplier
Additive Constant
100
1.00
0.00
Bunch Factor
I
I
I
I
V
strument Conditions:
pillary SC -
Instrument :VARIAN
Column : .2SMM
Column Length : 30M
Carrier Gas s HE
Flow Rate : 20CM/SEC
Split Ratio :
Temperature : 160
Injection Temp.: 200
Detector 1 : 300
Detector 2 :
Notes :
3400
ID .25UMFILM
RTX3
LINEAR VELOCITY 15 F'SI
1/MIN TO 230
tal Number of Peaks Detected* 46
Ret Time
^min]
1.62
1.80
5.69
7. 16
8.09
9.32
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L CuV-sec3
*********
Peak Ht
CuV3
Raw Amount
ug\L
215568.05 431136.09 183862.00 215568.05
000276
1302256.73
846.50
248.00
848.00
3452.37
2.60e6
1693.00
496.00
1696.OO
6904.73
96131.67
182.12
50.69
128.68
389.91
1302256.75
846.50
248.00
848.00
3452.37
-------
9.90
10.26
11. 54
13.21
13.87
14.53
16. 03
16.22
16.85
17.76
18.46
19.75
20.24
20.66
21.02
22.41
22.73
23.75
24.67
26. 03
26.49
26.98
27.39
29. 43
30. 10
30.48
31. 14
s-» • /
•jo .98
34.53
-^•5. wO
36.82
39.05
42. 47
42.81
46. 50
57. 20
60.21
61. 37
PCB1232
^ , 0'
DBC
2179.42
13455.66
163.25
0.00
434.50
6789.00
887.93
1509.50
20181.50
7583.50
4174.00
160.00
3041.96
3203.67
4245.91
4510.39
4733.86
6932.00
1498.00
237.98
2800.63
5133.37
6662.-37
377.25
6343.71
572.25
1133.81
606.18
571.00
1029.00
614.75
1664.51
348.50
1106.30
297.40
914.64
344.00
459.00
1363.75
0. 00
4358
jj.q% 50
'. uo
13578.00
1775.85
3012^00
8348.00
320.00
6083.92
6407.34
8491.81
9020.77
9467.72
; / .<• f
2996.00
475.96
5601.27
10266.73
13324.73
754.50
12687.42
1144.50
2267.63
1212.36
1142.00
2058.00
1229.50
3329.02
697.00
2213.00
594.81
1829.23
688.00
913.00
2727.50
63736.00
341.98
1327.12
39.56
914.88
70. 14
757.04
181.64
196.00
2037.57
867.89
612.13
36.21
422.93
430.83
387.38
676.62
568.35
800.63.
194.02
37.57
401.17
739.07
801.09
41.50
863.77
82.60
159.43
95.38
86.95
163.12
94.77
253.53
68.54
152.94
53.95
141.80
55.95
37. 33
260.43
5912.12
2179.42
13455.66
163.23
0.00
434.50
6789.00
887.93
1509.50
20181.50
7583.50
4174.00
160.00
3041.96
3203.67
4245.91
4510.39
4733.86
6932.00
1498.00
237.98
2800.63
5133.37
a662.37
¦377. 25
6343.71
572•25
1133.31
606. 18
571.00
1029.00
614.75
1664.51
348.50
1106.50
297.40
914.64
344.00
459.00
1363.75
0. 00
Total Area = 3369002.25
Total Concentration = 1641484.1250
Report by Doherty Bresnahan
000277
-------
r Maaa 1 C:\2700\8C3\)CF3012.rai» Data' 8/29/89 9s 18 AH Pap 1 of 1
tart Ti«t» 0.00 ain End Tiaf 70.00 ain Loh Pointt S104 uV High Point: 189075 uV
Meal Scali Factors 0.00 Plot Qffwts 0 aV Plot Scalts 100 aV
Chrotatograa
Ml
I
I J* tus53??3;s 3S 3 s e it
11M
23.33
3101
TIm (ain)
54,33
000278
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
PCB1242
laaaaaaasaaaasaaaa
Time : 8/29/89 9:20 AM
Study : MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range '• 1000
Data Acquisition Time: 8/28/89 10:57 PM
Delay Time
En d T i me
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
70.00
1.0
min.
min.
pts/sec
Ci \2700\GC5\MCF5013. raw
C:\2700\GC5\MCF5013.rst
C:\2700\GC5\F0E.ins
C:\2700\6C5\EXSTD.pre
C:\2700\GC5\MCC1242.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
: 0.00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold s 100
Mu11 i p1i er : 1. 00
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PSI
160
200
300
1/MIN TD 230
Total Number o-f Peaks Detected: 54
Ret Time
Cmin D
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L CuV-sec3
*********
Peak Ht
CuV]
Raw Amount
ug\L
1.62
1.81
8.07
9.32
9.90
10.25
103842.61 207685.22
745721.69 1.49e6
0002*79
459.25
1388.38
1424.64
10698.52
918.50
2776.75
2849.27
21397.03
92757.36
51465.13
81.62
162.44
216.59
1068.89
103842.61
745721.69
459.25
1388.33
1424.64
10698.52
-------
11.34
i^« 20
13.87 PGB12#"2-&^>
14.52
16.02
16.20
16.84
17.74 -P06 lO-fa-
lS. 43
18.92
19.73
20.23
20.64
21.00
22.38
22.71
23.72
24.64
23.33
26.00
26.46
26.94
27.36
28.33
29.43
30.07
0 • 43
31.09
32.32
"?T
¦ dm 4^
33. 93
34.46
33.27
36.77
-»'9 .
38.99
42.43
42.76
44.26
46.47
49. 14
49.90
32.69
33.49
57. 19
60.21
61.37
Q&O
63.24 -©66—Q&
797.99
19043.67
0.00
12821.30
1703.86
3131.30
37962.33
13464.88
10810.38
2830.80
714.98
6233.36
6511.12
8067.00
8887.04
9172.16
13979.67
2939.11
371.00
565.06
5928.30
10269.92
13598.84
1160.70
12727.04
1223.36
2341.19
1302.26
193.50
1270.44
2367.13
1241.00
3661.00
786.30
146.00
2389.50
372.10
2181.83
295.00
659.00
637.50
217.00
421.00
196.50
998.00
1463.30
32498.00
0.00
1395.98
2234.00
25643.00
3407.73
6263. Oi"
21620.77
5701.59
1429.95
12470.72
13022.24
16134.00
17774.08
18344.31
s8/o.
742.01
1130.13
11836.59
20339.84
25454.08
2450.73
4682.38
2604.32
386.99
2340.88
4734.23
2482.00
7322.00
1373.00
292.01
5179.00
1144.20
4363.70
590.00
1318.00
1275.00
434.00
842.00
393.00
1996.00
2927.00
64996.00
747.00
109.42
797.99
1377.39
19043.67
166.39
0.00
1447.99
12821.50
370.11
1703.86
381.34
3131.50
3786.24
37962.33
1692.06
13464.88
1309.32
10810.38
329.97
2830.80
104.77
714.98
872.94
6235.36
897,94
6311.12
799.62
8067.00
1314.06
3887.04
1093.44
9172.16
1610.70
13979.67
397.91
2939.11
68.67
371.00
90.04
563.06
844.68
5928.30
1488.07
10269.92"
1606.41
13598.84
111.28
1160.70
1742.34
12727.04
180.06
1223.36
323.48
2341.19
204.18
1302.26
36.24
193.50
189.07
1270.44
356.44
2367.13
206.41
1241.00
559.86
3661.00
139.88
786.50
30.74
146.00
365.16
2589.50
102.29
572.10
339.68
2181.35
40.32
293.00
105.99
659.00
110.88
637.50
45. 12
217.00
77.77
421.00
34.92
196.50
174.90
998.00
273.46
1463.50
5968.11
32498.00
63.84
0.00
3tal Area » 2236006.75
lotal Concentration = 1126312.8750
Report by Doherty Sraanahan
000280
-------
FileNaaa : C:\2700\H3\MCF5013.rM Data: 8/29/89 9:21 AH Page 1 of 1
Start Tiati 0.00 tin End Ti«a» 70.00 ain Lou Points S124 uV High Point: 96014 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 aV Plot Scale: too aV
Chiciatograi
1MH
ns>A
an ftgsos.sis assusfc asRts ;:t t t 7, *
««« s SSSCSI RGKKEJI »HB*« ? 5 S T B 6 8 8
S
i ^
a
«i
ft
3J3-:
MKhz
m
Trrinttnfffimwniiiriifiiiiiiiiiiii 11—711111 mi iiii 11 ml
111"
<117
11.(7
23.33
35.01
Tim* (nn)
3.33
000281
-------
Nelson Analytical 2700 Chromatography System Report Header
>amp le Name
sample Number
Operator
PCS1248
Time
Study
8/31/8? 10!SO AM
MCFARLAND
Inter-face # : 5
AutaSampler : None
Rack/Vial : O/O
Channel
attached
A/D mV Range s 1000
Data Acquisition
De1ay T i me s
End Time s
Sampling Rate :
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Times
0.00
70.00
1.0
8/29/89
min.
min.
pts/sec
11 AM
C•\2700\GC5\MCF3014.raw
C *\270O\GC5\MCF5014A.r st
C!\2700\eC5\F0E.ins
C:\2700\6C5\EXSTD.prc
C:\2700\SC5\MCC124a.smo
C:\2700\8C5\MCF54A.seq
In,j. v'olume
Sample Amount
2 uL
1.0000 units
Area Re.iact
0. 00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold : 100
Multiplier : i.00
Additive Constants 0.00
E'unch FjctOf'!
Instrument Condi t ionst
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sol it Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PS!
160
200
300
1/MIN TO 230
Total Number of Peaks Detected* 58
F:et Time
C m i n 3
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
'.tq\L CuV-secJ
*********
Peak Ht
C uV ]
Raw Amount
uq\L
1
1
10
U
62
32
26
51
13. 17
14.53
000282
143038.72 286077.44 116677.09 143038.72
'82969.63
258.00
181.75
8837.75
6059.51
1.56e6
516.00
363.50
17675.50
12119.02
>743. 28
47.08
27.68
719.64
654.60
•32969.63
253.00
181.75
8837.75
6059.51
-------
16. 03
16.85
17.78
18. 46
18.95
19.74
20. 23
20.65
21.00
22. 40
"7
23.73
24.64
25.34
26.02
26. 46
26. 94
27.36 Otb |24£
23. 25
29. 43
30. 08
30. 44
3 i. 09
31.'73
(y* < y
\0s
¦
255.00
31974.16
9370.27
6657.25
3514.02
849.47
10787.00
10040.14
13589.87
14705.70
10920.51
22701.16
4304.86
274.50
929.66
12329.74
19152.49
27638.13
1857.81
23414.69
2798.48
5757.91
4099.74
144.00
510.00
18740.55
13314.50
7028.05
• 1698.94
21574.00
20080.23
27179.73
29411.41
21841.
3509. 72
549.00
1859.31
24659.43
61.34
61.71
. 21
O-J
64.06
68. 70
"4011. 75
1466.50
0.00
688.25
306.50
11515.31
3199.48
-ob • C
3*.. "-<2
39^.75
7=4.50
3165.21
6--,*j,0. 4 c*
33. 92
3831.67
11663.34
34.45
3801.75
7603.50
35. 27
36.75-FCB124b Grf
9813.00
19626.00
0. 00
57 46•00
33.29
553.92
1107.84
33.97
8089.50
16179.00
40. 49
551.50
1103.00
41 . 53
228.75
457.50
42. 40
1488.85
2977.70
42. 75
"738 1. 09
14762.19
44. 22
609.25
1213.50
4o .43
2384.99
4769.95
46. 73
271.00
542.00
49. 1 1
6o7.00
1334.00
49.87
360.00
720.00
50.50
40 1.00
802.00
cr i, cr
J— • O-J
634.50
1269.00
53. 47
373.25
7 46.50
56. 13
144.75
289.50
57. 15
2627.00
5254.00
60. 17
1469.50
2939.00
•.> • 0 0
924.00
1376.50
613.01
60. 88
255•00
3082.99
31974. 16
905.05
9370.27
774.31
6657.25
368.51
3514.02
123.24
849.47
1439.13
10787.00
1388.01
10040.14
1ww9.86
13589.87
2073.64
14705.70
1346.52
10920.51
2535.57
22701. 16
561.25
4304.86
50.63
274.50
138.57
929.66
1686.27
12329.74
2664.52
19152.49
3174.67
27638.13
225.79
1857.31
31 14.80
23414.69
409.23
279Q.48
737.33
e- ^ ir -r o i
•J / w / . 7 I
;*:e; .
40-39. 7 4
i ¦ 'Jo
1 , vlj
74.9©
397.25
467.34
' C" 4
i O J • *
975.72
5831.67
614.14
3801.75
1468.26
9813.00
416.73
0. 00
92.09
55-i. 92
1169.29
3089.50
98. 92
551.50
39.30
~ Iff
^_«.o • / u
250.65
1488.35
1139.48
¦'381.0?
3. 56
c>09, 25
35t.31
2394,99
271.00
119.49
667.00
70. 02
360.00
73. 90
401.00
111.31
634.50
66. 49
Iff
/ -J • _
28. 60
144.75
467.35
2627.00
283.24
146V.50
6238.42
34011.75
236.07
1466.50
84. 77
0. 00
95. 04
688.25
56. 94
306.50
Total Area = 2540929.25
Total Concentration = 1267129.6250
-------
FileNa* : C:\2700\S3\ICROU.riii 0»t«: 8/31/89 10:31 AH Pa
-------
Samp 1e Name
Sample Number
Operator
Interface #
AutoSampler
Rack/Vial
PCB12S4
S Channel
None attached
0/0
i line
Studv
8/31/8? 10:'
MCFARLAND
AM
A/D mV Ranqe
1000
Data Acquisition Times 8/29/89
De 1 ay Time : 0.00 mm.
End Time : 70.00 min.
Sampling Rata : 1.0 pts/sec
1s 25 AH
Raw Data File :
Result File 5
Instrument File:
Process File :
Sample File :
Sequence File :
C:\2700\GC3\MCF5015.raw
C:\2700\GC3\MCF5015L.rst
C:\2700\SC5\F0E.ins
Cs\2700\GCS\EXSTD.pre
C:\2700\GC5\MCC1234.smp
C *\2700\GC5\MCF3 4A.ssq
!nj. Volume
¦ample -¦•.-sount
2 uL
1.0000 units
urea He.isc:'
Noise Thresholds 1
Dilution Factor: 1.00
D i v i sor s 1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
1.00
0.00
:ur
:n Facsor:
3400
ID .2:
Instrument Conditions!
Capillary GC -
Instrument :VARIAN
Column s .25MM
Column Length *. 30M
Carrier Gas : HE
Flow Rats : 20CM/1
•Split Ratio :
Temperature : 160 1/MIN TO
In j ec 11on Temp.s 200
Detector 1 s 300
Detector 2 :
Notes i
iUMFILM RTX5
;EC LINEAR VELCCI"
:~o
15 PS I
Total Number of Peaks Detected!
Ret Time
C m i n 3
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount- Peak Area
u=t\L CuV-sec 3
*********
Peak Ht
C u V 3
Raw Amount
uq \ L
1.62
1.81
20. 66
21.28
22. 43
00028*:
0.00 37461.45
0.00 438305.53
0.00 18853.78
0.00 7737.98
0.00 2341.20
0.00 12523.00
24992.20
15819.95
1225.10
335.21
138.98
758.23
0. 00
0. 00
0. 00
0. 00
0.00
0. 00
-------
23.77
24.73
26.50
26. 99
27.51
28.28
29. 47
29.76
3Q. 11
30. 48
31. 12
31.94
trey
33. 25
33.95
48
, 84
30
78
, 06
,69
30 I°e<3»
I
40.
40.
41.
4
-------
FileNaae : C:\2700\Ga\MCR015.raw Date: 8/31/89 10:54 AH Paqa 1 of 1
Start Timet 0.00 ain End Timet 70.00 nin Low Point: 5083 uV Hiah Point: 30048 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mV Plot Scale: 100 aV
ChroMtograi
I
1MM •
R 9t XV 53 S %
sin u i
_ a
o.tn-9
I
u
n
%
iwrf
C7-1 1
" 3 |\
liiirirrTif^J^TTft^nifiiTifTriiiitrsjri i;i r;n :i!" t
• i' ¦
1U7
B
JL
i
9.S
23.33 35.00
Tiu (»in)
000287
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
EVALB
T ime
Study
8/29/89 i 0:17 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/V/ial
5 Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Times 8/29/89 Q:5t AM
Delay Time : 0.00 min.
End Time ! 70.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Samp 1e File
Sequence File
C:\2700\GC5\MCF5015F.raw
C:\2700\GC5\MCF5015H.rst
CJ\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C'\2700\GC5\MCCEVAL.=mp
CJ\2700\6C5\MCF54A.ssa
In.j. Volume
Sample Amount
2 uL
1.0000
-------
. 6.66
ENDRIN
0.00
56031.00
4533.08
0.00
40.57
214.50
429.00
33.47
214.50
41.07
000
0.00
1392.00
115.69
0.00
46. 01
DDT
0.00
63538.00
5361.11
0. 00
51.26
ENDKET0
0.00
3907.00
331.97
0.00
60. 22
1818.7S
3637¦50
349.51
1813.75
61. 38
DBC
0.00
53339.00
4892.36
0.00
Total Area = 415266.63
Total Concentration » 19331.3086
:sssass8
Report by Doherty Sresnahan
Q00280
-------
FiliNut < C:\2700\GC3\fCF501T.rw Oatfi 8/29/89 10S17AN Pap 1 o< 1
Start TiM> 0.00 ain End Tiaai 70.00 ain lot Point: 9028 uV High Point: 16744 uV
Vertical Scala Factors 0.00 Plot Offsat: 0 aV Plot Scala: 100 aV
Chromatogram
%
§
#1
U
11.(7 &S 35.01
, Tia# (aia)
000290
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
100/200 A
Time
Study
8/29/39 5:32 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
s
None
0/0
Channel
attached
A/D mV Range : 1000
Data Acquisition Time» B/29/99 4:17 PM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process rile
Same 1e File
Sequence File
In.i. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
68.97
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF3027a. raw
C:\2700\GC5\MCF5027B.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD. pre
C: \2700\GC5\MCF51A. smp
C:\2700\GC5\MCF54A. sea
2 uL
1.0000 UG/kg
1
1.00
1.0000
Are;. Re.iset : 0. «X>
Area Threshold : 100
Mu11 i p1i er ; 1.00
Additive Constant: 0.00
Bunch Factor
Instrument Conditions
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
"low Sate
zo1i t Rat l o
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 P5I
160 1/MIN TO 230
200
300
Total Number o-f Peaks Detected: 32
********** EXTERNAL STANDARD REPORT *********
Ret Time Component Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin] Name ug\L CuV-secJ CuV] ug\L
12.37
3-BHC
33.09
355367.50
18737.06
93.09
13. 15
HPTCHLR
108.34
210396.00
11356.03
108.24
21.43
ALDRIN
35.34
368311.00
22524.74
35.34
26.05
HEPEF0X
94.57
265676.97
17471.43
94. 57
30. 39
END01
000291
93.74
247216.50
17366.3 7
93. 74
33.33
DIELDRIN
255.80
363847.16
26642.34
255.80
-------
167.36
234.19
137.87
1066.73
233.01
ttal Area = 3254795.00
tal Concentration = 2571.0537
J port by Doherty Bresnahan
38.12 END02 167.36 393028.00 23909.16
41.00 ENDALD 234.19 220685.34 16772.72
45.98 DDT -1-37.37 216690.22 19038.90
55.92 METHOXY 1066.73 394182.00 36343.93
61.32 DBC 238.01 228886.50 21127.40
000292
-------
FileMiia : C:\2700\GC3\HCF5027a.ra* Date: 8/29/89 5:33 PH Pagt 1 of 1
Start Ti«: 0.00 ain End Tina* 68.97 sin Lot Point: 5214 uV High Point: 41647 uV
Vertical Scale Factor: 0.00 Plat Offset: 0 nV Plot Scale: 100 aV
Chroiatogra*
S Rft
o rs*i
s 9 t>£ s?s ?
9 s II KS B HO 3
?3S
S| -9 SI
Mill
u
11
5
0.18-
3.S-3
lltt-3 "
¦frfV-
rfr-f'-rifVir
nrrrr
i-r«f f
i
Jt-
* 3
¦ »
3 2
1 S
r. .*11
1L« 22.3! *.« 45.» 57.47
Til* (ila)
4
000293
-------
I ample Name
ample Number
Operator
Nelson Analytical 2700 Chromatography System Report Header
i
[
iter-face #
nutoSampler
ack/Vial
EVALB
5 Channel
None attached
0/0
Time
Studv
8/30/89 3:05 AM
MCFARLAND
A/D mV Range
1000
ata Acquisition Times 8/30/89 12:54 AM
Delay Time
rnd Time
amp ling Rate
Raw Data File
Result File
I Tstrument File
•ocsss File
Sample File
J"eQuence File
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5033.raw
C:\2700\GC5\MCF5033.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCCEVAL.smp
C:\2700\GC5\MCF54A.seq
f
n j . Volume
Sample Amount
f
oise Threshold
Dilution Factor
i v i sor
2 uL
1. 0000
\
1.00
1.0000
Area Re.iect
Area Threshold
Multiplier
Additive Constant
'JO
100
1 . 00
0. 00
Bunch Factor: 1
nstrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
I
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
2CCM/SEC LINEAR VELOCITY
(¦ ; 3w ta-
5»lit Ratio
Tempera bura
Injection Temp.
Detector 1
Detector 2
Notes
otal Number o-f Peaks Detected: 13
¦>3 I
160 1/MIN TO 230
200
300
f:et Time
C m i n ]
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area Peak Ht Raw Amount
uq\L CuV-sec] C uV ] uq\L
1 . 60
1. 84
>1.47 ALDRIN
24.58
r-4.51 DDE
*•6.65 ENDRIN
G00294
1215.90
13248.3?
0. 00
685.00
0. 00
0.00
2431.79
26496.73
183396.00
1370.00
917.50
79735.50
1494.77
933.74
12354.55
101.19
59.81
6307.80
1215.90
13243.39
0. GO
635.00
0. 00
0. 00
-------
40.50 2366.57 4733.14 296.36
41.07 DDD 0.00 15BS.B6 111.51
45.98 DDT 0.00 50654.00 4530.83
50.56 5002.13 11764.25 103.52
51.23 ENDKETO 0.00 7004.73 442.39
60.20 2656.75 5313.50 499.52
61.37 DBC 0.00 69368.00 6395.22
Total Area = 444771.(56
Total Concentration = 26054.7305
Report by Doherty Bresnahan
2366.57
0. 00
0. 00
5332.13
0.00
2656.75
0.00
00G295
-------
FileNaM : C:\2700\GCS\nCF3033.riw Data: 8/30/89 8:03 AH Paga 1 of 1
Start Timet 0.00 ain End Tiui 70.00 sin Lom Point: 5213 uV Hiah Point: 17568 uV
Vertical Scale Factor: O.OO Plot Offset: 0 aV Plot Scale: 100 mV
Chrotatogra*
UUHH
«. *
r S 8
M S
St
3S
am-
bjjH
'AM-
11.67 23.33 35.00 48.67 58.33
Ti*e (Bin)
0002OH
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number-
Op era tor
Inter-face #
AutoSampler
Rack/Vial
100/200 B
5 Channel
None attached
0/0
T ime
Studv
3/31/89 12:33 AM
riCFARLAND
A/D mV Range
1000
Data Acquisition
Delay Time
End Time
Samp 1ing Rate
Raw Data File
Result File
Instrument File
Process File
Samp 1e File
Sequence File
T ime:
0. 00
63 « '-'0
1.0
8/30/89
min.
min.
p t s/sec
11:52 PM
C:\2700\GC5\MCF5039i. raw
C:\2700\GC5\MCF5039i. rst
C:Y2700\GC3\F0E.ins
C:\2700\GC5\EXSTD. pre
C:\2700\GC5\MCF51B. smo
C: 2700\GC5\MCF34A.
I n ..i. 7 a 1 ume
S amc 1 e Amou.n t
2 uL
1.0000 UG/kq
Noise Threshold
Dilution Factor
Divisor
1
1. 00
1.0000
Area Threshold
Multip1ler
Additive Constan'
100
1. 00
0. 00
•Bunch Factor-
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flew Kate
ScIit Ratio
T ~mo er a t ur e
I n ,i ac t i on Temp
Detector 1
Detector 2
Notes
3400
ID . 25UMFILM
VARIAN
. 25MM
301*1
HE
20CM/SEC LINEAR
- CI- - L,
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 33
Ret Time
Cmin ]
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
uqv>L CuV-sec]
Peak Ht
C u'v ]
Raw Amount
u.q\L
10.23 A-BHC
11.90 B-BHC
14.06 D-BHC
21.39 ALDRIN
28.85 G-CHLDANE
30.80 A-CHLDANE
000297
93.46 441920.00
96.01 150262.00
100.79 350087.69
96.37 390024.50
97.53 328867.00
93.43 323979.34
26227.36
S845.55
22337.30
26663.67
24368.64
24459.90
=>5. 46
96. 0 1
100.7°
96. 37
97.55
95. 43
-------
34.38 DDE 190.66 566213.00 46770.93 190.66
136.52 ENDRIN 324.39 283805.00 22039.67 324.39
40.29 DDD 276.33 292701.63 23646.67 276.33
44.41 ENDOSULFATE 195.97 356473.50 27852.94 195.97
51.04 ENDKETO 306.87 317000.00 25482.56 306.87
¦ 61. 18 DBC 334.78 253417.00 22417.21 534.78
™al Area = 4054750.50
otal Concentration = 2210.6040
i_
^ort by Doherty Bresnahan
000298
-------
FilsNi* : C:\2700\GC5\HCF5039i.ran Dat» 8/31/89 12:59 AH Paqe 1 of I
Start Tio#i 0.00 ain End Tiaes 63.30 ain Lqm Point' +958 uV High Point: 51476 uV
Vertical Scale Factor! 0.00 Plot Offset: i) aV Plot Scale: 100 aV
ChroMcogra*
UWH
a s » 3 a s i! t* ssi & a a s s c t
** !: si; s is » tuti : : :• s
a w
6 za
tt»-2
•xmr-.
**.*+* m
3
a
•c;o-5
(•a*-3
3-4*-
i I
•' i i1
iV { h
2 i
I I
•M II 1 I
J) it il 11 '
II II I • I I I I I
17r^iliii ii ii iiii Mill tiil i l*TP?'
ii «i i I n iiii
[ i
i i
n i
4*-*-
U
3 S
JU.
10.S
ZLia
31.65
Ti«e (sia)
42.20
52.75
000239
-------
Nelson Analytical 2700 Chromatography System Report Header
Simple Name
.Ample Number
perator
Interlace #
JutoSampler
Rack/Vial
100/200 A
5 Channel
None attached
0/0
Time
Studv
8/31/39 12:13 PM
MCFARLAND
A/D mV Range : 1000
I
ata Acquisition Time! 8/31/89 1:06 AM
elay Time
End Time
amplinq Rate
«
aw Data File
°3suIt File
Instrument File
,-ocess File
¦sample File
~=quence File
|r. . Vo 1 Limi?
sample Amount;
Ioise Threshold
ilution Factor
n i visor
Instrument Conditions:
capillary GC -
Instrument
Column
Column Length
Carrier
-low Rate
cp i, 1-3 Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5043.raw
C:\2700\GC3\MCF3043.est
C:\2700\GC3\FGE.ins
C:\2700\GC3\EXSTD.prc
C: \2700\GC3\NCF31A. ship
C:\2700\GC3\MCF34A.sea
2 uL
1.0000 UG/kg
1
1. 00
1.0000
Ar e a Re ,:ect : 0. 00
Area Threshold '• 100
Mu11 i p 1 i er : 1.00
Additive Constant: 0.00
Su.nch Factor:
7ARIAN 3400
.25MM ID .25UMFILM PTX5
30M
' HE
20CM/SEC LINEAR VELOCITY 11 P3I
160 1/MIN TO 230
200
300
I
otal Number o-f Peaks Detected: 34
I
et Time
C m i n ]
Componen t
Name
EXTERNAL STANDARD REPORT *********
Adjusted Amount Peak Area Peak Ht
up vL CuV-sec] CuV3
Paw Amount
uq ¦- L
12.36 G-BHC
13.12 HPTCHLR
21.46 ALDRIN
26.03 HEPEPOX
30.34 END01
33.77 DIELDRIN
000300
91.34 370461.30
113.69 224182.00
90.07 336447.00
101.45 283001.00
99.76 263070.00
276.09 392701.84
19671.99
12705.06
22971.63
19045.39
18249.64
29239.27
91.34
115.69
90. 07
101.43
99. 76
276.09
-------
33.05 END02
40.92 ENDALD
45.38 DDT
35.81 METHOXY
61. 19 DBC
130.19
247.14
159.36
1233.88
271.35
412398.00
232884.38
250466.22
455948.00
260952.00
30870.06
17585.11
21782.11
40637.35
23087.36
180.19
247.14
159.36
1233.88
271.35
Total Area = 3534511
Total Concentration
= 2866.8120
Report by Doherty Bresnahan
Q00301
-------
FileNua : C:\2700\GCS\nCF3043.rw Date: 8/31/89 12:14 Ftt Page 1 of 1
Start Tims 0.00 sin End Tia«: 70.00 ain Lom Point: 3069 uV High Point: 45642 uV
Vertical Scale Factor: 0.00 Plat Offset: 0 aV Plot Scale: 100 aV
Chiotatograi
1N.I
0.3J-
*«K
aaH
it tn_3 ^
5 ii
5 sa " 83 3 * C.ilSS * 5,a SS6; SfJ.i
355 ; i; sua an** ? Rtma
T
I a I til
.1. il ii II
M ~ TTilnniTTrr^iri'rraif!
( in > ' (<
iS § I r § i 8 x
a s 3, s ? ,*, 3 ?
11.W 23.33 3. DO *.W 58.3
Ti&e ruin)
000302
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
PBLK-1
Lab Name: LOCKHEED-ESC
Contracts 68-03-3249
Lab Codes Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 0 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.: SDGi No.:
Lab Sample ID: 9S187RB
Lab File ID:
Date Received: 7-23-89
Date Extracted: 7-31-89
SONC Date Analyzed: "I
Dilution Factor: 10
CONCENTRATION UNITS:
UQ/kq Q
319-84-6
319-85-7
319-86-8
58-89-9
76-44-8
309-00-2
1024-57-3
959-98-8
60-57-1
72-55-9
33213-65-9
72-54-8
1031-07-8
50-29-3
72-43-5
53494-70-5
5103-71-9
5103-74-2
8001-35-2
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
t1096-82-5
-alpha-BHC 160
-beta-BHC 160
-de 1 ta-BHC 160
-gamma-BHC (Linaane) 160
-Heptach lor 160
-A 1 dr in— 160
-Heptach lor epoxide 160
-Endosul -fan I 160
-Dieidrin 320
-4, 4'-DDE 320
-Endrin 320
-Endosul-fan II 320
-4,4' -DDD 320
-Endosul-fan sulfate 320
-4, 4' -DDT 320
-Methoxych lor 1600
-Endrin ketone 320
-alpha-Ch lor da.ne 160
-gamma-Chlordane 160
-To'/aphene 3200
-Aroc lor-1016 1600
-Aroc lor-1221 1600
-Aroc lor-1232 1600
-Aroc lor-1242 1600
-Aroc lor-1248 1600
-Aroc lor-1254 3200
-Aroc lor-1260 3200
U
U
U
U
U
U
U
!J
U
U
U
IJ
U
IJ
u
u
u
u
u
u
U
u
IJ
u
FORM 1 PEST
1/87 Rev.
000303
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : PBLK1
Sample Number: 9S187RB
Operator :
Time
Study
8/30/89 1:27 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
12:48 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR018.raw
e:\pkd\MCFR018.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e: \pkd\clpa. snip
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0. 00
*****EXTERNAL STANDARD REPORT*****
ssssssssssssssssa:ssssas=ssss=ss=ss=sssssssss==sss:s===5=;=ss==ssssss
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Rat Tlaa Component Adjusted Amount Raw Amount Peak Area Peak Ht MULTIPLIER
[rain] Nam -UCAb— UG/L (uV-sec} [uV] Ad J/Raw
L.45
25.60 0BC 71.45 216.50 2.88e6 65203.52 0.33
Total Area - 2887785.75
total Concentration ¦ 71.4454
Report by Tim Rand, Lockheed-ESC
Q00304
-------
Chromatoqram
FilcNaae : e:\pkd\HCFR01B.rau Date: 8/30/69 1:27 PM Page 1 of 1 ^
Start Tiw: 0.00 ain End liae: 47.00 sin low Point: -1217S17 uw High Point: 2009310 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 «V Plot Scale: 250 ifiV
CN
2S0.000
200.333
166.667
125.000
41.667-
-0.000
7.83 l'j.67 23.50 31.33 39. 17
-------
Nelson Analytical 2700 Chromatography System Report Header
2:15 PM
Sample Name : PBLK1
Sample Number: 9S187RB
Operator ;
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
12:48 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR018.raw
e:\pkd\MCFR018A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 0.00
* * * * * EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
*at tin* Coopenant Adjuittd Amount Raw Amount Peak Acta Peak Bt MULTIPLIER
[mini Hum .—UC/L [uV-»«el tuVJ Adj/Raw
21.14 ESCOffll.FAIE - a tomn "n ¦¦jsi.os 8, a a— VCL
25.SO BBC 85.36 228.68 2.38*6 65203.52 9.33
Total Araa - 2990955.75
lotai Concentration • 39.1*08
Report by Tim Rand, Lockheed-ESC
000306
-------
Vertical Scale factor: 0.00 Plot Offset: 0 mV Plot Scale: 250 mV
•—" uS
CM CM CM
CLf
CD
cr>
OL>
250.000.
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
I I
Jc.-1
f i i"i f i i i i pT i it i i»t i r | i i i i i i i | i it i i i i i i | i i i
7.83 15.67 23.50 31.33
Time (min)
V H g
.g-P —
63
S
hi
i i i i i | i i i i i i i i i
39. 17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : PBLK-1
Sample Numbers 9S187RB
Operator :
Time
Study
8/29/89 9:47 AM
MCFARLANDl
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time:
Delay Time
End Time
Sampling Rate
8/29/89
0•00 m i n.
70.00 min.
1.0 pts/sec
2:39 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File s
Inj. Volume :
Sample Amount
Noise Threshold
Dilution Factor
Divisor
C:\2700\GC5\MCF50ISA.raw
C:\2700\GC5\MCF5015A.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C: \2700\GC5\MCF54A. seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject : 0.00
Area Threshold : 100
Multiplier : 0.33
Additive Constants 0.00
Bunch Factor: 1
Instrument Conditionss
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sp 1 i t Rat io
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
eg I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 11
EXTERNAL STANDARD REPORT
Ret Time Component Adjusted Amount Feik Area Peak Ht Raw Amount
Cmin] Name .-«iTXtT\, CuV-sec] CuV] uq\L
-5-1.51
nLDniN
o. i;*8—
—1 07 i 00
i 26 *
55.79
MCTI10XV
2*7'?
2609,50—
—195.16
61.37 DBC 94.77 247029.00 16455.54 256.88
MV
Total Area = 251059.50
000308
-------
Total Concentration = 87.2627
Report by Doherty Bresnahan
0003D1
-------
FileNaw : C:\Z700\6C5\MCF3013A.rw Data: 8/29/89 9:47 AH Paga 1 of I
"Lvt Tim 0.00 sin End Tiax 70.00 iin low Point: 4893 uV High Point: 88844 uV
I "tical Seals Factor: 0.00 Plot Offset: 0 aV Plot Seals: 100 aV
™ Chmatograa
I
1NJI
ILS}-:
9SSH
asfi
l 5
TOT
* 1 m
* i| n
* • -
ft
x
t—rr
>i it
X
1117
1 | | 1 I j
i i r. i i ?i i 9 [ i it i rii
as
35.00
Til*
-------
_Nelson Analytical_2700 Chromatography System Report Header
Sample Name : PBLK-1
Sample Number: 9S187RB
Operator :
Inter-face #
AutoSampler
Rack/Vial
T ime
Studv
8/29/99 1:59
MCFARLA.ND
PM
5 Channel
None attached
0/0
A/D mV Ranqe : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Time: 8/29/89 2:39 AM
0. 00 m in.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5015A.raw
C:\2700\GC5\MCF5015E.rst
C:\2700\GC5\FOE.ins
C:\2700\GC3\EXSTD.prc
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
Ini. Volume
Sample Amount
2 u.L
1.0000 UG/kq
Area Reject
0.
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow R.afee
SpI11 Rat io
T emperature
In.iectian Tsmp
Detector 1
Detector 2
Notes
Area Threshold
Mu 11 i p1i er
Additive Constant
100
0. 33
0.00
Bunch Factor
3400
ID .25UMFILM RTX!
VARIAN
. 25MM
30M
HE
20CM/SEC LINEAR
VELOCITY 15 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 11
EXTERNAL STANDARD REPORT
Ret Time Component Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin] Name CuV-sec] CuV] u.g\L
14. 34-
D DilC
0. 03 334. 00
29.03
0. l'j
Jl.-jr
MLUM'tP*
'J • [J r IV /' ^
o"7->
61. 37
DBC
107.69 247029.00
16453.54
326.34
Total Area = 249784.00
000311
-------
| tal Concentration = 107.8505
J[port by Doherty Bresnahan
000.31*:
-------
FileNaa* : C:\2700\GC3\HCF50l5A.raw Date: 8/29/89 1:59 PM Pag# I of I
Start Tinas 0.00 ain End Tines 70.00 Bin Loh Point: 4893 uV High Point: B6844 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 aV Plat Scale: 100 sV
Chroiatogras
11
II
5
3b
n i
j * i
. u
i S!
a
- ». »
a » s
3
*
*
a
9
£
*
9
II
s
1U7
23.33
35.00
4U7
tt.33
TiM (unj
Q003I3
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
fcPA SAMPLE NO.
F'BLK-2
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Cods: Case No. :
Matrix! (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOU
'/. Moistures not dec. O dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
3AS No. : — SDG No. :
Lab Sample ID: 9S197RB
Lab File ID*
Oata Received! 7-25-99
Date Extracted: 8-1-89
SONC Date Analysed:
Dilution Factor: 10
CONCENTRATION UNITS:
ug/kg Q
319-84-6
319-85-7
319-86-8
58-89-9
76-44-8
309—00—2
1024-57-3
959-98-8
60-57-1
72-55-9
72-20-8
33213-65-9—
72-54-8
1031—07—8
72-43-5
53494-70-5—
5103-71-9
5103-74-2—
8001-35-2
12674-11-2-
11104-28-2-
11141-16-5-
53469-21-9-
12672-29-6-
11097-69-1-
11096-82-3-
-a 1 pha-BHC ISO U
-beta-BHC 160 U
-de 1 ta-BHC 160 U
-gamma-BHC (.Lindane) 160. U
-Heptachlor 160 U
-Aldrin 160 U
-Heptachlor epoxide 160 U
-Endosul -fan I 160 U
-Dieldrin 320 U
-4,4' -DDE 320' U
—Endr in 320 U
—Endosul-fan II 320 U
—4, 4' -DDD 320 U
—Endosul-fan sul+'ate 320 U
— 4,4'-DDT 320 U
—Methoxychlor 1600 U
—Endr in ketone 320 U
—alpha-Chlordane 160 U
—gamma-Ch lor dane 160 U
—Toxaphene 3200 U
—Aroc lor-1016 1600 U
—Aroc lor-1221 1600 U
—Aroc lor -1232 1600 U
—Aroc lor-1242 1600 U
—Aroc lor-1248 1600 U
—Aroc lor-1254 3200 U
—Arocloi—1260 3200 U
FORM 1 PEST
1/87 Rev,
000314
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : PBLK2 Time : 8/30/89 1:29 pm
Sample Number: 9S197RB Study : MCFARLAND
Operator :
Interface # : 2 Channel : B A/D mV Range : 10000
AutoSampler : Varian 8000 without controller
Rack/Vial : 255/255
Data Acquisition Time: 8/30/89 1:39 AM
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File : e:\pkd\MCFR019.raw
Result File : e:\pkd\MCFR019.rst
Instrument File: e:\pkd\pkd.ins
Process File : e:\pkd\pextstd.prc
Sample File : e:\pkd\clpa.smp
Sequence File : e:\pkd\MCFRLND.seq
Inj. Volume : 2 uL Area Reject : 0.00
Sample Amount : 1.0000 uL
~~~~~EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
•
Ret Tim Coopooant Adjusted Amount Raw Amount P«*k Arcs Peak Ht MULTIPLIER
[mini Him UC/L [uV-j«cl [uV] Adj/lUv
ta.t* OHBOliD 1.91 S-rM ¦0000.08 ia8>.18 M)
25.62 DBC 73.72 223.39 2,97.6 66010.27 0.33
Tool Ar»» - 3019722.73
Total Concentration - 74.7260
Report by Tim Rand, Lockheed-ESC
000315
-------
Chromatogram
filename : e:\pkd\MCFR019.raw Date: 8/30/89 1:29 PH Page 1 of 1
Start Tine: 0.00 Bin End liae: 47.00 nin Lou Point: -2105297' uV High Point: 101S940 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 OV Plot Scale: 250 mV
c
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : PBLK2 Time : 8/30/89 2:17 PM
Sample Number: 9S197RB Study : MCFARLAND
Operator :
Interface # : 2 Channel : B A/D mV Range : 10000
AutoSampler : Varian 8000 without controller
Rack/Vial : 255/255
Data Acquisition Time: 8/30/89 1:39 AM
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File : e:\pkd\MCFR019.raw
Result File : e:\pkd\MCFR019A.rst
Instrument File: e:\pkd\pkd.ins
Process File : e:\pkd\pextstd.prc
Sample File : e:\pkd\clpb.smp
Sequence File : e:\pkd\MCFRLND.seq
Inj. Volume : 2 uL Area Reject : 0.00
Sample Amount : 1.0000 uL
»EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
Rac Tina Cooponant Adjuatad Amount Raw Amount Peak Araa Ptak He MULTIPLIER
[mlnj Naaa Uc/L [uV-»ael ;uv| AdJ/Raw
ei.io DiiDOQWirotD o.tfl iq.63 io?om «« .piai i.33
23.62 DBC 88.03 256.91 2.97.4 66030.27 0.33
vk.
Total Araa • 31*7572.73
Total Coneanttatien » 9a.2270
Report by Tim Rand, Lockheed-ESC
000317
-------
Chromatogram
Filename : e:\pfcd\HCFR019.rau Date: 6/30/69 2:17 PH Page 1 of 1
Start liae: 0.00 Bin End liae: 47.00 ain Lou Point: -2105297 uV High Point: 1016940 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mV Plot Scale: 250 mV
cd
250.000
166.667
Of
125.000
-0.000
7.83 15.67 23.50 31.33 39.17
Time (min)
-------
Nelson Analytical 2700 Chromatography System Report Header
Samp 19 Name :
Sample Number:
Operator :
Inter-face #
AutoSamp lor
Rack/Vial
PBLK-2
9S197RB
S > Channel
None attached
0/0
Time
Study
8/29/89 9:49 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition Time: 8/29/89 3:54 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noi9e Threshold
Dilution Factor
Divisor
0.00 min.
70.00 min.
1.0 pts/sec
C:\2700\GC3\MCF5015B.raw
C:\2700\GC5\MCF5015B.rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51A. smp
C:\2700\GC5\MCFS4A. seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject : 0.00
Area Threshold : 100
Mu11 i p1i er : 0.33
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Co1umn
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN
. 2SMM
30M
HE
20CM/SEC
3400
ID .25UMFILM
RTX5
LINEAR VELOCITY 15 RSI
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected) 11
Ret Time
Cminl
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
un Vfc *1^/^ CuV-secl
Peak Ht
CuV:
Raw Amount
ug\L
21.36 ALDHIN
34.59 DICLDniN
37.91 ENDQ2
-<>.04-
0. 15-
501.00
636.00
40 ¦ 20
0.12
r6+-
419Q.40
—04.09
209.53
O. 45
1.03 A
55.03 METH0XY
61.45 DBC
Sr^4 3069« 00 220.21
177.52 517312.00 33732.22
0.31 l»
537.93
000319
-------
|'tal Area - 525716.50
otal Concentration = 181.0503
Report by Doherty Bresnahan
000320
-------
FilaNua : C:\2700\GC3\NCF3013B. raw Date* a/29/89 9 M9 AH Paga 1 of 1
Start Tia«< 0.00 tin End Tiaai 70.00 ain Lou Point* 5065 uV High Point: 80882 uV
Vertical Seals Factor» 0.00 Plot Offset: 0 aV Plot Scalai 100 aV
ChxoutograB
lMH
ttat-j
I
I 5U
s.rH
ii
S 5
X ft
T~rr
1
ILff
23.3} 35.06 4.W
TiM (axa)
m 5
n » s*
¦mmf
if I | I s I i i e ! h
,1* ¦ , * ft. I I I I r ¦ 191 , 1-1 ¦ Hi I I T i | i M
000321
-------
Nelson Analytical 2700 Chromatography System Report Header
I imp I e Name
imple Number
Operator
I iter-face #
TjtoSampler
Rack/Vial
F'BLK-2
9S197RB
5 Channel
None attached
0/0
Time
Studv
8/29/89 2:01 PM
MCFARLAND
A/D mV Range
1000
I
\ta Acquisition Time: 8/29/89 3:54 AM
belay Time
End Time
| imp 1ing Rate
Raw Data File
Jjesult File
¦ istrument File
¦ ¦acess File
Sample File
iequ.ence File
I
0.00 m i n.
70.00 min.
1.0 pts/sec
C: \2700\GC5\MCF3015B.raw
C:\2700\GC5\MCF5015F.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.prc
C:\2700\GC5\MCF5IB. smp
C:\2700\GC5\MCF34B.seq
i i. Volume
Sample Amount
fjise Threshola
dilution Factor
1 i v i sor
i
2 uL
1.0000 UG/kg
1
1. 00
1.0000
Area Re.iset
Area Threshold
Mu11 i p1igr
Additive Constant
10<
Junch Factor
0. 00
istrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
"low Rate
Split Ratio
T emperature
I n i ec t i on Temp
Detector I
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM PTX3
30M
HE
20CM/SEC LIHEAR VELOCITY
160 1/MIN TO 230
200
300
I
otal Number ot Peaks Detected: 11
EXTERNAL STANDARD REPORT
I
et Time Component Adjusted Amount Peak Area Peak Ht Paw Amount
[min] Name Cu.V-ssc] CuV] ug\L
21. 36 hLDRIN 0. 04¦ SO 1. 00 40.20 0.12 '• '>
34 . 59 DDE u~6.00 34.00
371 91 CNDRIN 4100, 40 209.53 *¦» 00 :,i
61.45 DBC 225.52 517312.00 53732.22 683.40
otal Area = 522647.50
000322
-------
Total Concentration = 227.2181
Report by Doherty Bresnahan
000323
-------
FileNue : C:\2700VSCS\f1CF5015B.raw Data: 8/29/89 2:02 Pfl Pag* 1 of 1
Start Tine: 4.00 nin End Ti«e: 70.00 ain Low Point: 5065 uV High Point: 80882 uV
'Vertical Seals Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 oV
Chroaaiograi
5
ji
ai
01
8 5
ft ft
1 * tf
H fc sa
rr
I 1! Ill'
u -
11 - 5 o
M ^ , ,5
—T—
58.33
11.67 23.33 3.00 tt.W
Tiae (ain)
000324
-------
ID
PESTICIDE ORGAN ICS ANALYSIS DATA SHtET
tF'A SAMPLE
OFOIMS F'REG PC
Lab Name: LOCKHEED-ESC
Contract: 68-03-149
Lab Code: Case No. :
Matri::: (soil/water) SOIL
Sample wt/vol: 30 grams
Levels (low/med) LOW
7. Moisture: not dec. 1.9 dec.
E:: trac t ion :
GrC Cleanup: '.Y'/N) N pH:
CAS rJO.
COMPOUND
SAS No. i SDG No. :
Lab Sample ID:
Lab File ID:
Date Received: 7-25-39
Date Extracted: 7-31-39
30NC Date Analv:eds * '"j4--" ^ 1
C11 >j. ticn F ac t or: l C
CONCEN f'RATION UN ITS:
ug/ki Q
1^ 1*5 ^
319-34-6
319-85-7
319-96-3
58-89-9
76-44-8
309-00—2
1024-57-3
959_og_g
1 .-«j-
72-54-3
1031-07—9—
30-29-3
53494-70-5-
5103-71-9—
5103-74-2—
8001-35-2—
12674-11-2-
11104-28-2-
11141-16-5-
53469-21-9-
12672-29-6-
1 1097-69-1-
11096-82-5-
-alpha-BHC 32 U
—beta-BHC 32 U
-del ta-BHC 82 U
-gamma-BHC (Lindane; 32 U
-Heptachlor 32 U
—Aldrin S2 U
-Heptachlor epoxide 32 L!
—En dosu.lt an I 32 U
— Dieldrin 163 U
-4, 4'-DDE 163 U
— Endosu.l -fan II la3 'J
—4,4'-ODD 163 J
—Endosul-fan sul+ate 163 U
—4, 4'-DDT 163 U
—Metho::ych lor 315 U
—Endrin ketone 163
—alpha-Ch lor dane 82
—gamma-Ch lordane 82
—Toxaphene 1631
—Aroc lor-1016 815
—Aroc lor-1221 315
—Aroc 1 or-1232 315
—Aroc lor-1242 : 315
—Aroc lor -1243 315
—Araclor-1234 1631
—Aroc lor-1260 1631
U
u
u
IJ
'J
u
u
u
u
IJ
IJ
FORM 1 PEST
« / r-i t .
k f O / i» 0 v
-------
Nelson Analytical 27 00 Chromatography System Report Header
1:31 PM
Sample Name : OFOIMS Pre-GPC
Sample Number: 9S185MS
Operator :
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
2:30 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR0 2 0.raw
e:\pkd\MCFR0 2 0.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
>EXTERNAL STANDARD REPORT*****
Instrument ID:
Varian
3400-1
GC Column
ID: 2250/2401
¦
Ret Tlma
Component
Adjusted Amount Raw Amount
Peak Area
Peak He
MULTIPLIER
[min)
Hum
UC/L
tuV-see]
[uVl
AdJ/Raw
3. J1
G-BHC
46.46 6&.33
1.60*6
177940.98
3.68
4.32
HPTCHLR
50.86 74.80
1.62*6
143254.70
0.68
5.20
ALDRIN
48.64 71.53
1.65*6
124347.70
0.68
11.22
DIEU3RIN
218.93 321.96
6.96*6
184391.83
°-68 \l/
0.68
17.62
DOT
ill <»** 384.04
3.29*6
93006.38
0.68
23.73
DBC
146.ii 213.68
2.87e6
62938.97
0.68
Total Ar«» • 18108400.00
Total Concentration ¦ 773.4702
Report by Tim Rand, Lockheed-ESC
000328
-------
Chromatogram
FileNane : e:\pfcd\MCFR020.raw Date: 8/30/89 1:31 PN Page 1 of 1
Start Tiae: 0.00 ain End Km: 47.00 Bin Low Point: 5250 uV High Point: 345090 uV
Vertical Scale factor: 0.00 Plot Offset: 0 wM Plot Scale: 250 mV
250.000
208.333
rrr.^r-f
-0.000
7.83 15.67 23.50 31.33 39.17
-------
Nelson Analytical 2700 Chromatography system Report Header
Sample Name : OF01MS Pre-GPC
Sample Number: 9S185MS
Operator :
Time
Study
8/30/89 2:19 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate ; 1.0 pts/sec
2:30 AM
Raw Data File ;
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume ;
Sample Amount ;
e:\pkd\MCFR020.raw
e:\pkd\MCFR020A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
; 0.00
*EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tin
[mini
CaopoMusc
Hum
Adjusted Aoouist Saw Amount F**k Arc* P**k He MUIKPLIER
- /js. UC/L (u¥-i«el [uV] AdJ/IUw
5.20 ALPRIH
I, B
11.22 ODE
13.21 EH0KXH
,,,31 7n nwrniat-
23.73 BBC
45.24
»¦!*»•
66.51
1.6S«6 12414J.J0
237.21
142.52
t.M
148.87
209.51
6.96*6 184191 II
2.91*6 104219.39
1.83 moe.aa—
HiW-
*16833.Si II
173.23
257.69
2.87*6 6293S.97
3.68
} 68
3,68
-r-w-
».»»
3 .si
%-
Total Aim « 13023474.00
Total Concentration - 619.1240
Report by Tim Rand, Lockheed-ESC
000328
-------
Date: 8/30/89 2:19 PH Page
FileNane : e:Vpkd\HCFK020.rau - . .
Start Tiae: 0.00 aio End Tfae: 47.00 ain Lom Point: 5250 uV High Point: 345090 uV
Vertical Scale factor: 0.00 Plot Offset: 0 M Plot Scale: 250 mV
Chromatogram
1 of i ^
cr
<=>
eox.
CO
a->
CXL
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
c
o
o
CJ
pj-ooo-
CD
- i rs i^s C>* C*s« «qr
Cn S ts S ovj u-i
r-J u>' od zz Z2 td
V
II
M
o —in
•— -*r in
cn rs CN
. r'n f ;"n
i r^i f3! i i i i^f i i*t
7 .83
15. 67
23 . 50
31.33
39.17
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number:
Operator :
Inter-face #
AutoSampler
Rack/Vial
MS pre-gpc
9S185MS
5 Channel
None attached
0/0
T ime
Study
8/29/89 9:32 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition Times 8/29/89 5s08 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
mxn.
min.
pts/sec
C:\2700\GC5\MCF5015C.raw
C:\2700\GC3\MCF5015C.rst
C:\2700\GC5\F0E.ins
Cs\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject J 0.00
Area Threshold : 100
Multiplier : 0.68
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 49
EXTERNAL STANDARD REPORT
Ret Time Component Adjusted Amount Peak Area Peak Ht Raw Amount
[min] Name CuV-sec3 CuV] ug\L
12.40 G-BHC * 37.38 222941.00 12109.79 55.27
18.IS HPTCHLR 42.23 120340.00 6828.33 62.10
21.54 ALDRIN 39.35 248296.88 15326.87 57.87
27.04- MCPCPQX 0. 36 147Sr00 04. 58 0. 65 *>'
-50. 49 ENDQ1 0. 16 1792. 06 100. 61 0. 69 (f\\
33.92 DIELDRIN 126.44 264467.91 19356.97 183.93
D00330
-------
I
30¦ 23 END02 e*-38 1277.23 76.2* 0.D6 i/
41.10 CNDALD 2-r£3 2010i72 lQOiGl 2i9Q t-»
46.08 DDT 121.99 281975.13 24063.91 179.40 U
55.07 MCTIIOXV : 3-^75 2037. 00 143.71 5t54— ^
61.42 DBC 165.92 234651.00 18852.60 244.01
Total Area = 1382067.25
Total Concentration = 540.4901
Report by Doherty Bresnahan
000331
-------
rileHMt : C:\2700\GC5\HCF301SC.rin Data: 8/29/89 9:53 AM Paga 1 1
Irt Tint 0.00 ain End Tiaai 70.00 ain Low Point: 5203 uV High Point: 33384 uV
tieal Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Chroiatograa
1MH
* *5 a a* « ?s t i a3S3 anzsssn s* s s *. 63 sw C *
'• «•: : • 5 8 U Ma SUM MS* J 5 $ S P UK IS I 9
I
i
a.n~.
iusH
sur!
s.cH
_ I ii ii iiiL 11 irlrr i
i iiiiiihiii nVwrnrn
\ t I * £ § £ ! .
ii, i» i 11 i*. i i r. I1?, i f i r*i , i »|
Ir-i
11.(7 23.33 35.00 44.(7 5i33
Tis« (ain)
000332
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : MS
Sample Numbers 9S185MS
Operator s
T ime
Studv
8/29/89 2:04 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5 Channel
None attached
0/0
A/D mV Range
1000
Data Acquisition Times 8/29/39
Delay Time : 0.00 min.
End Time : 70.00 min.
Sampling Rate : 1.0 pts/sec
08 AM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5015C. raw
C:\2700\GC5\MCF5015I.rst
C:\2700\GCS\FOE.ins
C:\2700\GC5\EXSTD.pre
C: \2700\GC5-\MCF51B. smp
Cs\2700\GC5\MCF34B. seq
Ini. Volume
Sa.mp 1 e Amoun t
2 uL
1.0000 UG/kq
Area ft=.iect
0.0'.'
Noise Threshold
Dilution Factor
Divisor
1
1. 00
1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
0.63
0.00
Bunch Factor
Instrument Conditionss
Cap i1lary GC -
Instrument
Column
Column Length
Carrier Gas
Flaw Pate
'5p 1 i t Rat io
T emperature
Injection Temp
Detector 1
Detector 2
Notes
3400
ID .25UMFILM RTX5
VARIAN
. 25MM
30M
HE
20CM/SEC LINEAR VELQCIT"
15 PS I
160
200
300
1/MN TO 230
Total Number o-f Peaks Detecteds 49
EXTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount
L-V—
Peak Area
[u.V-sec 3
Peak Ht
CuV]
Raw Amount
u.q \L
101, 30
-fr-
-frH€
—12Q0i 00
01?. "0
13 ¦ uG
-shg
a. 2i
1
7e;
i
I
21.54
-59. 01.
ALDRIN
0 CHLD0NE
31.00 A CIILDAHC
41.72 243296.d8
0.-24 1166. 00
_0.IS 71G.OO
13326.37
as.65
73. 31
6i.
000333
-------
34.61 DDE 81.96 357932.34 28188.66 120.53
36.76 ENDRIN 168.12 216304.22 16379.51 247.23 f
-40. 02 DDD 7.21 11229. 00 ~29. 10 10. £0—
*4.03 CNDOGULrATC 6Q4. 99 71.24 0.30—
•51.31 CNDKCTO 7.-43 11269. 00 901: 46 10.91—^
61.42 DBC 210.79 234651.00 13852.60 309.99
otal Area = 1085732.00
otal Concentration = 518.7329
eport by Doherty Bresnahan
000334
-------
FileNaaa : C:\2700\GC3\nCF3015C.rui Data: 8/29/99 2:03 PM Page I of 1
Start Tiaai 0.00 ain End Time: 70.00 ain Low Point! 5203 uV High Points 33384 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 #V Plot Scale: 100 aV
Chxcautograa
1N.W-:
aa-i
5I*K
» >xn a » s ssa asssss* :? ^ ^ s a
:• 8 It tx» R BR RMS? J 5 : ji ( !!« u I a
:«sH
i a
I
3
1 *
li
'IVrfS
< I t
I
l~ff—I!!: :i ii iWi n niiniitnTHftrHrnn ; li'i ,i'n'i ii,in nfrm—-
m
j # i
¦ u ¦
1 H i? !
1 ,
I 3
, 'i
lit?
23.33 S.M
ii | i i i
1
tt.33
Til* (mia)
000335
-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHtET
tF'A SAMPLE NO.
QFOIDS PREGPC
Lab Name: LQCKHEED-ESC
Contract: 63-03-3249
Lab Code: Case No. :
Matrix: (soil/water) SOIL
Sample wt/voi: 30 grams
Level: (low/med) LOW
Moisture: not dec. 1.9 dec.
Extraction: (SepF/Cont/Sonc)
SPC Cleanup: (V/N) N pH:
CAS NO.
COMPOUND
SAS No. : SDS No. :
Lab Sample ID: 9S186DS
Lab File ID:
Date Received: 7-25-89
Date Extracted:. 7-31-89
SONC Date Analysed:
Dilution Factor: 10
CONCENTRATION UNITS:
ug/kg Q
319-84-6
31?-65-7
3 1 ?-S6-5
53-3?-®
76-44-3
309—00-2
1024-57-3
959-98-8
60-57-1
72-55-9
72-20-8
33213-65-9—
72-54-8
1031-07-8—
72-43-5
53494-70-5—
5103-71-9—
5103-74-2
3001-35-2
12674-11-2—
1 1 104-23-2-
11141-16-5-
53469-21-9-
12672-29-6-
11097-69-1-
11096-82-5-
-alpha-BHC
-beta-BHC
-de 1ta-BHC
-gamma-BHC (Lindane;
-Hep tach 1 or .
-A1dr in
-Heptachlor epoxide
-Endosul -fan I
-Dieldr in
-4,4'-DDE
-Endr in
-Endosul-f an II
-4,4'-DDD
-Endosul-fan suit ate
-4,4'-DDT
-Methoxycnlor
-Endrin ketone
-a1pha-Ch1 or dane
-gamma-Ch1 ordane
-T oxaphene
-Aroclor-1016
-Aroclor-1221
-Aroclor-1232
-Aroc1or-1242
-Aroclor-1243
-Aroclor-1254
-Aroclor-1260
o?
_/ ^
IJ
32
U
32
U
82
u
32
u
32
u
32
u
82
u
163
u
163
u
163
u
163
IJ
163
u
163
u
< t
IJ
315
IJ
163
u
32
•J
32
IJ
1631
u
315
u
315
¦J
315
IJ
315
u
815
u
1631
u
1631
u
FORM 1 PEST
1/37 Rev.
Q0033«
-------
Nelson Analytical 2700 Chromatography System Report Header
1:34 PM
Sample Name : OFOIDS Pre-GPC
Sample Number: 9S186DS
Operator :
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
3:23 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File
Sequence File
Inj. Volume :
Sample Amount :
e:\pkd\MCFRO 21.raw
e:\pkd\MCFR021.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
R«t IlM
Coopo&aac
Adjuatad Amount Raw Amount P«ak Araa Paak He MULTIPLIER
(min)
Na»
UG/L
[uV-««c)
[uVl
AdJ/Raw
3.31
G-BHC
• "60. M
39.01
2.38«ft
236136.32
0.68
4.32
HPTCHLR
63.28
96.00
2.38a«
188893.73
0.68
3.20
ALORIH
61 . 34
90.20
2.08«6
137333.34
3.68
11.20
0IELDRIH
261.69
384.84
3.32*6
223430.19
0.68
13.*9
END02
3.37
4. 96
139030.27
1300.43
0.68
17.36
00T
j. 7/ J2J. JJ." •
• 473.81
J.. 06«6
117049.33
0.68
23.61
DBC
219.71
323.10
-.10*6
76923.96
0.68
Total Area • 2310*884.00
Total Concentration ¦ 993.4631
Report by Tim Rand, Lockheed-ESC
A
000337
-------
Chromatogram
Filetfaae : e:\pkd\HCFR021.rau Date: 8/30/09 1:14 PH Page 1 of 1
Start line: 0.00 ain End liae: 47.00 ain Low Point: 5920 uV High Point: 678230 uV
Vertical Scale factor: 0.00 Plot OffMt: 0 aV Plot Scale: 2S0 mV
CO
if*
250.000
208.333
166.667
125.000
IPTT,
-0.000
7.83 15.67 23.50 31.33 39.17
Time (min)
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : OFOIDS Pre-GPC
Sample Number: 9S186DS
Operator :
Time
Study
8/30/89 2:21 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2 Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0 pts/sec
3:23 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File
Sequence File :
Inj. Volume :
Sample Amount :
e:\pkd\MCFR0 21.raw
e:\pkd\MCFR021A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT
Instrument ID: Varian 3400-1 GC Column ID: 2250/2401
R«t Tlaw
Caapoaarvt
Adju»t*4 Amount Raw Amount
Pailt Art*
P«»k Ht
MULTIPLIER
[mini
Nm».
UC/L
UC/L
[uV-s«e|
[uV]
AdJ/Raw
S.20
AL0KIN
57.03
83.89
2.08(6
157533.34
0.68
8.37
G-CHLDANE
0.32
0 . 1*7
961.0.00
351.58
0.68
11.20
DDE
283.36
417.01
3.32*6
225450.19
0.68
13.18
ENDUH
93.8*
138.00
1.91*6
68290.50
0.68
13.49
000
6.12
9.00
139030.27
3500.45
0.68
21.03
EHDOSULFATE
27.00
39.71
357933.00
3643.90
0.68
23.61
0BC
262.31
386.04
4.30*6
76923.96
0.68
Tool Ar*» - 17147396.00
Tool Concentration • 730.3897
Report by Tim Rand, Lockheed-ESC
00033??
-------
Chromatograra
FileNane : e:\pkd\MCFR02t.rau Date: 8/30/69 2:22 PH Page t of t
Start Tlae: 0.00 ain End Tiae: 47.00 Bin Lou Point: 5920 uV High Point: 67B230 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 raV
250.000
208.333
166.667
125.000
•0.000
i r i
7.83 15.67 23.50 31.33 39.17
Time (min)
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Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
Inter-face #
AutoSampler
Rack/Vial
OFOIDS F'REGPC
9S136DS
5 Channel
None attached
O/O
T i me
Studv
9/1/39 2:26 AM
MCFARLAND
A/D mV Ranqe : 1000
Data Acquisition Time: 8/31/S9 11:04 FM
Delay Time
End Time
Sampling Rate
0.00
70.00
1.0
m in.
m in.
pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MC2010.raw
C:\2700\GC5\MC2010.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF2A.smp
C:\2700\GC5\MCF2CA.seq
[r, j. Volume
3 smp1e Arnounz
2 uL
1.00*50 UG/kq
A r & 3. P a j c
Noise Threshold
Dilution Factor
D ivi sor
1
1.00
1.0000
Area Threshold
Flu 11 i p 1 i er
Additive Constant
100
0. 63
0. 00
bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Co 1umn
Column Lanqth
Carrier Gas
Flow Pats
3clit Ratio
Temperature
I n .1 sc t i on Tamp .
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
2CCM/SEC LINEAR VELOCITY 15 F":
160 1/M IN TO 230
200
300
Total Number o-f Peaks Detected: 49
EXTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount Peak Area Pgak Ht Raw Amount
CuV-sec] CuVj ug'^L
12.37 G-BHC
13. 13 HF'TCHLR
21.47 ALDRIN
30.jG CNOQl
33.32 DIELDRIN
33.11 END02
14.67 73315.50 9932.13
63.83 191021.00 11819.32
56.34 239192.03 19006.17
204.
21.53
93. 37
C-®
'Wta i W ^
I
191.54 467115.72 36814.06
0.55 1378,.^110.06
3nr
231.67 /
0.81
-------
JgNDftLD
45.95 DDT
~ S. 7'?>—METHOX Y-
*.11
206.90
—13. 2&
S370.72
317112.00
6040.no
*11.25-
28990.86
456.11
j i 0 0
304.26
19.80
318.45
2^
61.24 DBC
216.54 300420.00 25960.80
I
I
tal Area = 1657118.50
tal Concentration = 769.3851
sort by Doherty Bresnahan
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FileNut : C:\2700\GC3\HC2010.ra* Date: 9/1/99 3:27 AH Page 1 of 1
Start Tinas 0.00 ain End Tines 70.00 tin Low Points 5214 uV Hi«h Points 51576 uV
Vertical Scale Factor: 0.00 Plot Offset: o mV Plot Scale: 100 «V
Chrasatograi
»* »
t !3 a*S=t« if,
fc OH*RMS :c
s?» *6 3
JrS fifi a
8
a
I si
l
TFT?i : i :r ;W^r~^nTfbfVflP'»i''i i'nin ;i; ;rnr
I * ^ - I a 3
1 | sj Sjjj
¦1 I ¦ ¦ I* I i'i I I I I r l"l I I- I fl
11.67 3.33 3.00 H.il
Time (ain)
«.33
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Nelson Analytical 2700 Chromatography System Report Header
| > mp1e Name : OFOIDS PREGPC
sample Number: 9S186DS
,per a tor :
i
Time
Study
9/1/89 S:46 AM
MCFARLAND
iter-face #
AutoSampler
nek/Vial
I
5 Channel : A
None attached
0/0
A/D mV Range J 1000
?jita Acquisition Time: S/31/39 11:04 PM
Delay Time
Itd Time
amp ling Rate
Raw Data File
I3SUIt File
Tstrument File
Process File
iaiTio Is File
¦^queries File
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MC2010.raw
C:\2700\GC3\MC201OA.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.prc
C:\2700\GC5\MCF2B.smo
C: \2700 v» G C 5\M C F 2 C 3. seg
I
riTiple Amount:
..oise Threshold
Dilution Factor
|„,o,
instrument Conditions:
t~sp i 11 ar y GC -
Instrument
Column
Column Length
C:. <.! 6
73.26
0.3?
-1r'r>
21.47 ALDRIN
20. "5" d-CHLDftNC
10.93 A-CHLDftNC
I
—
-------
34.50
36.65
DDE
ENDRIN
108.39 399391.23
221.52 363173.73
33363.35
28434.11
159.40
325.76
4
1
• CT 1 1 ¦
CMm/CTn
u•83 1338.uu
32. 34
1 .
1
61 . 24
DBC
220.90 300420.00
25960.30
324.85
Total Area = 1383602.50
Total Concentration = 620.4094
Report by Doherty Bresnahan
-------
! C:\2700\GC3\MC2010.ran
t Time: 0.00 ain End Tia»: 70.00 ain
ical Scale Factor: 0.00 Plat Offset:
DjU: 9/1/89 8U7 AH Paw 1 of 1
Low Paint: 5214 uV Hiah Paint: 51576 uV
0 aV Plat Scale: 100 aV
ChroMtograi
*6? I a«:n 2*
a; rn mm s8R K fS HRRRMS 55
lil
3
rp» fit. 3
s.»-
;».»-§
a
*-= 1
S
I 3
II!
11
•mi 11 ifi>ii irT^r"!roflrftTtor »i'i 'if.ji ;ii iVnr
11
? <£ 3 | 5 5 - 8 o § | o
AM Li n 3,- 5 'm—I r-L
11.67
23.33
35.00
Tia* (tin)
#>.U
38.33
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