Environmental Monitoring
Systems Laboratory
P.O. Box 93478
Las Vegas, NV 89193-3478
>EPA
Research and Development
MC FARLAND STUDY
McFarland, California
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600R90021
December 1990
X-RAY FLUORESCENCE SITE SCREENING SURVEY,
SOIL SAMPLING, AND CHEMICAL ANALYSES
MCFARLAND, CALIFORNIA
by
Lockheed Engineering and Sciences Company
Las Vegas, Nevada
Prepared for
K. R. Scarbrough
Superfund Technology Support Center
Environmental Monitoring Systems Laboratory-Las Vegas
Las Vegas, Nevada 89193-3478
Contract Numbers
68-03-3245, 68-03-3249, and 68-C0-0049
ENVIRONMENTAL MONITORING SYSTEMS LABORATORY-LAS VEGAS
OFFICE OF RESEARCH AND DEVELOPMENT
U.S. ENVIRONMENTAL PROTECTION AGENCY
LAS VEGAS, NEVADA 89193-3478

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NOTICE
This technical assistance report has undergone a technical and/or
quality assurance review and approval by personnel of the EPA/ORD Environ-
mental Monitoring Systems Laboratory at Las Vegas (EHSL-LV). It is for
internal Agency use only. Distribution, application, and use of the data
contained herein are at the discretion of Regional personnel.
ii

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CONTENTS
Summary	iv
Introduction	1
Results 		A
Conclusion 		6
Appendix 1 - X-ray Fluorescence Screening Survey	Al
Appendix 2 - Soil Sampling	B1
Appendix 3 - Inorganic Chemical Analyses	CI
Appendix 4 - Semi-Volatile Chemical Analyses	D1
Appendix 5 - Pesticide Chemical Analyses	El
iii

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SUMMARY
This report presents the results of a McFarland, California field
portable x-ray fluorescence (FPXRF) site screening survey, soil sampling, and
chemical analyses performed by the U.S. Environmental Protection Agency (U.S.
EPA) Environmental Monitoring Systems Laboratory-Las Vegas (EMSL-LV) and U.S.
EPA Region 9 Emergency Response Team (ERT). EMSL-LV participated in this
activity and prepared this report at the request of U.S. EPA Region 9 and the
California Department of Health Services (CDHS). The on-site screening survey
was conducted in July 1989 and laboratory analyses were conducted during
August and September 1989.
A high incidence of childhood cancers reported from the McFarland,
California area prompted the request for a survey to help determine metal
levels in soil. A FPXRF field screening survey was conducted to identify
potential areas of arsenic, lead, and chromium contamination. Soil samples
were collected from areas of elevated metal contamination as indicated by the
FPXRF for subsequent EMSL-LV laboratory analyses. The EMSL-LV laboratory work
included limited analyses for pesticides, heavy metals, and semi-volatile
organic compounds.
This screening survey was designed and intended to provide insight into
areas of potentially high levels of contamination. Given the study objectives
and design, sampling methodology, and use of field screening instruments to
measure soil contamination, the various concentrations of metals should be
interpreted only in a relative sense. This means that individual concentra-
tions can be judged as relatively higher or lower than other study concentra-
tions measured by the same instrument. This is an important characteristic of
the screening data and should be carefully considered in drawing conclusions
from the study.
Taking into account that the study was a screening survey only, and that
the results are levels of contamination that are useful in judging relative
concentrations among study samples, certain inferences may be drawn. A major
inference is that no unusually high levels of heavy metals were detected in
the screening survey. Certain sample locations, such as in a railroad ditch
and near a potato washing pit, were, by the nature of the land use activity,
automatically expected to yield higher levels of certain metals, and the
screening survey confirmed this. Other areas, however, judged in relative
terms among themselves, were not unusual, and do not suggest unusually high
concentrations of metals or pesticides.
It is necessary, should absolute measures of contamination be desired,
that site-specific soil standards be prepared in advance of a second round of
field measurements. Also, all FPXRF instruments must be pre-calibrated to
these standards and to one another to insure data comparability.
iv

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INTRODUCTION
McFarland, California is a small agricultural community (popula-
tion 5150) located in the San Joaquin Valley, 22 miles north of Bakersfield
(Figure 1). A high incidence of childhood cancers reported in this area
prompted the California Department of Health Services (CDHS) and Region 9 to
request the assistance of EMSL-LV in conducting a field portable x-ray
fluorescence (FPXRF) field screening survey to determine metal levels in soil.
The EMSL-LV assistance provided to Region 9 and CDHS included FPXRF site
screening, soil sampling, and laboratory analytical chemical services. The
intent of the FPXRF survey was to identify potential areas of heavy metal con-
tamination in the soils at McFarland. If elevated soil levels were detected
by the FPXRF, soils in these areas would be collected and sent to EMSL-LV for
pesticide screening, heavy metal, and semi-volatile organic compound analysis.
The primary inorganic contaminant of concern identified by the CDHS was
arsenic, because of its long-term use in arsenic-containing pesticides at
and/or in the vicinity of McFarland. In addition, the FPXRF team also per-
formed on-site screening analyses for lead and chromium. These FPXRF measure-
ments were performed at grid locations identified by personnel from the CDHS
(Figure 2).
SITE SURVEY
The site survey was a combined effort of CDHS, Region 9, and EMSL-LV
personnel. The CDHS designed a sampling grid approach (Figure 2). This
sampling grid-configuration consisted of identifying 400 x 400-foot interval
locations throughout the McFarland city limits. The north-south grid lines
were alphabetically labeled and the east-west grid lines were numerically
labeled providing a coordinate system identifying each sampling location. The
sampling location was identified by recording the number (east-west) first
followed by the (north-south) alphabetical identifier.
Once the grid was established, CDHS located the corresponding property
owner(s) and requested permission to sample on their property. If the pro-
perty owner denied permission, an adjacent property was selected for sampling.
The EMSL-LV FPXRF survey trailer was set up in the McFarland public pool
parking lot and used as a base station for the survey. It was also used as
the local public relations/news conference demonstration area for FPXRF
technology prior to the survey.
1

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FIELD PORTABLE X-RAY FLUORESCENCE INSTRUMENTATION
The FPXRF instrument used for this field survey was the X-MET 880. This
instrument is a field-portable, energy-dispersive XRF spectrometer marketed by
the Columbia Scientific Industries Corporation, Austin, Texas. The unit is
self-contained, battery powered, microprocessor based and weighs 8.5 kg. The
surface analysis probe is specifically designed for field use. The X-Met 880
is hermetically sealed and can be decontaminated with soap and water. The
probe includes a radioisotope source of Curium-244, a proportional counter and
associated electronics. The source is protected by an NRC-approved safety
shutter.
The electronic unit of the X-MET 880 has 32 calibration memories called
'models.' Each model can be independently calibrated for as many as six ele-
ments. These can be used to measure elements from silicon to uranium assuming
the proper isotope source is available. The unknown sample intensities are
regressed against the calibration curves to yield concentrations.
XRF is based on the principle that photons produced from an X-ray tube
or radioactive source bombard a sample to produce fluorescence. The incident
photons impinge on the electron cloud of the atom. This process creates
vacancies in one or more of the inner shells causing instability within the
atom. As the outer electrons seek stability by filling the vacancies in the
inner shells, the atom emits energies as X-ray photons. The emitted energy
(fluorescence) from a particular shell is characteristic of the atom in which
it was produced and is equal to the difference in bonding energy between the
outer shell electron and the vacant shell. Host elements under the photon
bombardment fluoresce simultaneously to produce a spectrum of characteristic
radiation. It is this spectrum that the detector senses and counts.
FPXRF SURVEY
The purpose of the McFarland study was to conduct an FPXRF survey to
identify elevated levels of heavy metals in McFarland soils. The original
plan was to survey McFarland with three FPXRF instruments. This would enable
the grid area to be covered in approximately 2 days. The instruments were to
consist of one from Region 9, one from EMSL-LV, and one unit borrowed from
U.S. EPA Region 6. However, due to mechanical problems with the EMSL-LV FPXRF
unit, a unit was borrowed from Columbia Scientific Industries Corporation in
Austin, Texas. The borrowed unit also had mechanical problems at the start of
the survey, therefore, the survey was limited to the Region 9 and Region 6
units. The Region 9 instrument was calibrated by the manufacturer and the
Region 6 instrument was calibrated to its previously surveyed site. Inasmuch
as the two instruments were not calibrated to each other, nor calibrated with
site-specific standards, all data obtained should be viewed in relative terms
only.
Two XRF teams, consisting of two individuals each, conducted the survey.
One member operated the unit while the other recorded the data. The teams
were assisted by a Spanish interpreter provided by CDHS. McFarland is
2

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bisected by State Route 99, which was used to divide the sampling area between
the two sampling teams. The Region 9 Team (Team A) sampled primarily east of
State Route 99, while the EMSL-LV Team (Team B) sampled west of the highway.
The Region 9 team started the survey by conducting a reference
(control/background) survey in the town of Delano, California (Figure 1).
This survey consisted of taking FPXRF measurements at sampling locations iden-
tified in Figures 3 and 4 at the Fremont and Del Vista schools located within
the Delano city limits. Delano was selected as a reference site because of
its habitat and agricultural similarities to the town of McFarland. At the
time of the survey, Delano was not identified as an area that had abnormal
instances of cancer. However, as reported in Special Report on Health (1990),
Delano has also been identified as a cancer cluster area.
At the request of CDHS, detailed FPXRF surveys were also conducted at
four additional areas of interest within McFarland city limits. The Region 9
team surveyed sample locations at the Montabello Rose Company, the Potato
Plant, and at Well No. 5 (Figures 5, 6, and 7 respectively), while the EMSL-
LV team surveyed sample locations at Veil No. 6 (Figure 8).
SOIL SAMPLING
The objective of this field sampling effort was to physically collect
soil samples, only if the FPXRF readings indicated that there were areas with
elevated concentrations of heavy metals. The laboratory analysis of collected
soil samples would provide a quantitative confirmatory analysis. To accom-
plish the confirmatory soil sampling phase, the sampling team arrived two days
after the start of the FPXRF field survey. This time interval allowed for an
assessment of field survey data to determine and identify potential soil
sampling locations.
No elevated heavy metals concentrations had been detected by the time
the soil sampling team arrived. It was decided, however, that a limited num-
ber of soil samples be collected to confirm the relative readings obtained.
One sample was collected from Delano's Fremont School to validate the readings
at the reference area. CDHS and Region 9 personnel also selected 16 sampling
sites in McFarland based on their knowledge of the area. The soil samples
were collected using standard soil sampling procedures, as identified in
Appendix 2, and labeled according to the nearest node on the FPXRF grid (see
Figure 2 to geographically locate nodes).
The soil sample identification numbering system was modified from the
FPXRF sampling identification system. The soil samples were labeled by
listing the alphabetic code first, followed by the numeric code and a two-
digit number identifying the order in which the sample was collected.
The collected soil samples were analyzed for metals, semi-volatile
organic compounds, and a limited number of pesticides. Metal analysis was
performed by a combination of 1) inductively coupled plasma emission spectro-
scopy and 2) flame, cold vapor, and furnace atomic adsorption spectroscopy.
Semi-volatile organic compounds were analyzed by gas chromatography/mass spec-
trometry. Pesticide analysis was by gas chromatography. The results of these
analyses are presented in Tables 1, 2, and 3 with detailed information
provided in Appendices 3, 4, and 5.
3

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RESULTS
FPXRF SURVEY
The purpose of this screening study was to identify areas of potentially
high levels of metals or pesticides. The field portable XRF units were sepa-
rately calibrated with different sets of generic soil standards. Generically
calibrated XRF units are only able to generate relative data. This means that
any single number has no meaning by itself; it is not an absolute value.
Therefore, the data have been reported as simple instrument readings and these
relative values should not be compared to any absolute values, including those
with regulatory significance. Furthermore, without prior site-specific cali-
bration standards, there is no way to go back and determine any kind of
regression or scale that will yield absolute values from the FPXRF data
obtained at McFarland. The results from the FPXRF survey and more detailed
information on the FPXRF method are provided in Appendix 1.
SOIL SAMPLES
The soil samples were analyzed for 23 metals (Table 1). A cursory
statistical review of this data was conducted. Each of the 23 metals was
evaluated for the statistical parameters of the sum of all values (Ex), mean
(E), and standard deviation (SD)(an_1). Based on these values, three SD was
calculated and an elevated concentration was considered to be greater than the
mean value plus three SD (x + 3 * SD) (Table 4). If a non-detect (ND) for a
metal was listed, the analytical detection value was used in the calculations.
If a metal had a value that was considered elevated (greater than x + 3 * SD),
that value was considered an outlier and the statistical tests were recalcu-
lated omitting this value (Table 5).
The first cursory review indicated that sample M14A08 had elevated
levels of arsenic, copper, lead, and zinc; sample J212 had elevated levels of
mercury and vanadium; and sample D414 had elevated cadmium. The seven differ-
ent metals were reevaluated omitting the outliers, to see if they were skewing
the statistical results enough to mask other possible elevated metals. This
reevaluation showed that sample M14A08 also had an elevated level of mercury
and sample H709 had an elevated level of cadmium. However, all of the ele-
vated concentrations are well below the Total Threshold Limit Concentration
(TTLC) values from California Administrative Code, Title 22, Section 66699
(1990).
This evaluation did show that samples M14A08, J212, D414, and H709 all
have metal levels that do not statistically fit in the narrow "normal" range
4

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of the overall metal analysis. These samples were collected in the following
locations: the railroad ditch approximately 200 meters southwest of the Mon-
tebello Rose Company building (M14A08), the potato washing pit located north
of town (J212), near City Water Well #6 (D414), and the backyard of a house on
Second Street (H709). Laboratory data sheets for the metals analyses are
included in Appendix 3.
Soil samples were also analyzed for semi-volatile organic compounds
using gas chromatography/mass spectrometry. Two phthalate compounds, bis(2-
ethylhexyl)phthalate and di-n-butylphthalate, were detected in most of the
samples, but were also detected in associated laboratory blanks. Phthalate
compounds are used in plasticizers and are commonly detected as laboratory
contaminants. Otherwise, no other semi-volatile compounds on the Target Com-
pound List (TCL) were detected above their detection limit in any of the soil
samples. The sample from the railroad ditch (M14A08) was the only sample in
which TCL compounds, other than phthalates were identified at estimated con-
centrations below their detection limit. Ten polynuclear aromatic hydrocarbon
(PAH) compounds were identified in that sample at estimated concentrations
between 60 and 600 ug/kg. PAH compounds are common constituents of petroleum
products and creosote, both of which are associated with railroad operations
as fuel and a wood preservative for railroad ties. Semi-volatile compound
data sheets are included in Appendix 4.
Pesticide analyses by gas chromatography were also performed on the soil
samples. Only one pesticide (4,4'-DDE) in one sample (J212) was detected
above the Contract Required Quantification Limit (CRQL). The concentration in
this sample was 1057 ug/kg, which is above the California TTLC for DDE. Addi-
tional pesticide analytes were identified below their CRQLs in many of the
samples. The pesticides and their percentage of detection in the samples
include: 4,4'-DDE (94 percent), 4,4'-DDD (29 percent), 4,4'-DDT (88 percent),
a-chlordane (29 percent), and g-chlordane (29 percent). The detection limits
for the pesticide analyses were all below their California TTLC values, except
for Endrin with a detection limit of 320 ug/kg and a TTLC value of 200 ug/kg.
The pesticide results are provided in Appendix 5.
5

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CONCLUSION
Taking into account that the study was a screening survey only, and that
the results are levels of contamination that are useful in judging relative
concentrations among study samples, certain inferences may be drawn. A major
inference is that no unusually high levels of heavy metals were detected in
the screening survey. Certain sample locations, such as in a railroad ditch
and near a potato washing pit, were expected to yield higher levels of certain
metals. Analysis of collected soil samples confirmed this. Other areas,
however, judged in relative terms among themselves, were not unusual, and do
not suggest unusually high concentrations of metals or pesticides.
It is necessary, should absolute measures of contamination be desired,
that site-specific soil standards be prepared in advance of a second round of
field measurements. Also, all FPXRF instruments must be pre-calibrated to
these standards.
6

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reference
1. Special Report on Health, 1990. Clouds of Doubt. Special Report,
August 1990.
7

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DELANO
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MC FARLAND
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CALIFORNIA
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COUNTY
Figure 1.
8

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MC FARLAND SAMPLING GRID
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9

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FREMONT SCHOOL
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Figure 3.
10

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DEL VISTA SCHOOL
DELANO, CALIFORNIA
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11

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12

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POTATO PLANT SPECIAL AREA
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15

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TABLE 1. SUMMARY OF SOIL ANALYSIS RESULTS FOR METALS
McFARLAND, CALIFORNIA
DELANO CALIFORNIA
McFARLAND SAMPLES	SAMPLE	11LC
CHCH1CAL
M1t
0802
f 1204
H709
11205
J212
K411
L4A07
L513
H14A08
M4A06
M510
M116
P715
P803
R1417
Df 01 |
(mg/kg)
ALUMINUM
6440
8420
6600
8600
10400
18500
10300
8410
9820
14600
9830
8490
5070
11500
6850
8220
7230 |

ANTIMONY
ND(12.0)N0(12.6)ND(12.2)ND(12.0)ND(12.0>ND(12.0)
14.5 ND(12.0)ND(12.3)ND(12.0)ND(12.4)ND(12.6)HD(12.0)HD(12.1)ID(12.2)
13.9
ND(12.2) |
500
ARSENIC
2.0
2.4
14.1
3.3
3.8
7.1
2.6
2.6
8.3
254
2.8
1.9
2.1
2.5
1.9
2.4
2.3 |
500
BARIUM
67.3
IIS
102
85.8
123
190
104
99.8
115
198
110
96.6
55.0
98.4
148
86.4
113 j
10000
BERYLLIUM
0.67
MD(0.32)ND(0.31)
0.65
0.32
0.S4 ND(0.30)ND(0.30)
0.36
0.50
0.35 ND(0.32)ND(0.30)
0.80 ND(0.31>
0.32
NO(O.JI) |
75
CADMIUM
2.2
M)(0.84)ND(0.82)
1.7 ND(0.80)K)(0.80)M>(O.SO)IB(O.SO)ND(0.82)ND(0.80)ND(0.83)ND(0.64)IB(0.80)
1.4 ND(0.81)N0(0.80)
ND(0.82) |
100
CALCIUM
3760
7250
3570
3460
4570
4360
3220
2470
4160
7510
3760
3320
1640
3070
4260
2630
2960 |

CHROMIUM
17.J
14.7
28.3
16.6
16.5
27.8
13.8
12.5
15.3
27.7
15.2
12.9
11.3
24.7
13.7
15.3
11.6 j
2500
COBALT
12.2
7.1
6.S
8.7
6.9
12.5
7.1
7.1
6.8
12.4
8.1
6.1
4.0
13.3
5.8
7.2
6.0 j
8000
COPPER
15.5
12.7
1S.0
14.4
17.0
21.7
10.9
10.3
12.3
332
12.9
12.2
6.7
20.6
17.8
13.1
10.2 j
2500
IRON
9350
11600
9860
11900
14200
26600
13600
11900
14000
27600
13500
13100
7190
15400
10100
11700
10500 j

LEAD
6.2
8.0
86.7
31.1
96.3
14.5
12.2
S.3
8.S
222
7.5
15.6
26.5
8.7
72.2
16.6
9.9 |
1000
MAGNESIUM
2780
3980
3010
3610
4150
8160
4130
3830
4540
6640
4250
3670
2050
4370
2830
3380
3100 j

MANGANESE
178
249
223
228
284
313
270
240
244
491
292
243
156
355
226
305
238 j

MERCURY
0.16
V—
0
1
0.1S ND(0.14)
0.23
1.80 ND(0.14)ND(0.14)ND(0.13)
1.3
0.26 ND(0.14)M>(0.13)
0.25
0.37 N0(0.15)
0.15 |
20
NICKEL
8.9
9.9
10.9
15.5
19.9
18.9
12.1
12.5
9.4
32.3
11.9
9.5
7.5
20.3
15.0
13.8
20.6 j
2000
POTASSIUM
2730
3260
3620
4150
4980
7490
3710
3350
3480
5830
3820
3820
2160
4010
2710
3140
3490 j

SELENIUM
ND(0.40)ND(0.42)NO(0.41>ND(0.40)NO(0.40)K>(0.40>ND(0.40)ND(0.40)ND(0.41)ND(0.40)ND(0.41)ND(0.42)ND(0.40)IB(0.40)ND(0.41)ND(0.40)
ND(0.41) j
100
SILVER
2.2
1.1 M>(1.0)
2.2 ND(I.O) ND(I.O)
1.1
1.5 ND(I.O)
1.1
1.4 MD(I.I) *0(1.0)
1.6 10(1.0) ND(I.O)
1.6 j
500
SODIUM
368
663
380
483
400
518
S16
398
400
577
541
380
251
442
650
394
581 |

THALLIUM
ND(0.40)HO(0.42)ND(0.41)ND(0.40)ND(0.40)ND(0.40)ND(0.40)ND(0.40)ND(0.41)
1.3
0.48
0.46 ND(0.40)ND(0.40)ND(0.41)ND(0.40)
WH0.41) j
700
VANADIUM
26.4
31.2
26.5
32.5
28.8
64.5
29.8
28.5
33.6
48.5
33.7
26.7
17.1
39.5
23.4
29.4
27.9 |
2400
ZINC
48.2
43.0
97.8
58.2
131
128
36.9
35.5
49.4
477
38.0
63.0
30.1
48.9
131
40.8
34.2 |
sooo
ALL ANALYTICAL RESULTS EXPRESSED AS MG/KG.
NDC12.0) = CHEMICAL NOT DETECTED UITH DETECTION LIMIT IN PARANTHESES
TTLC (TOTAL THRESHOLD LIMIT CONCENTRATION) VALUES FROM CALIFORNIA ADMINISTRATIVE CGOE, TITLE 22, SECTION 66699.

-------
TABLE 2. SUMMARY OF SOIL ANALYSIS RESULTS FOR SEMI-VOLATILE
ORGANIC COMPOUNDS - McFARLAND, CALIFORNIA
NeMRytlB SAMPLES
compound
PHENOL
B1S(2-CHlOBOETKYl)ETHER
2-CHLOMPHENOL
1.3-oicmoaoaEiHmi
1,&-OICHLOaOBEHZ£ME
8EN2YL ALCOHOL
t,Z*DiCHU»OUUOa
2-iCTim.PMim.
Bisa-cmonoisopRommiiER
4-MEnm.MEWX.
n-nitsosodi-n-propuamihe
KiXACHLORQETNMU
NITROBENZENE
tSOnOMME
2-niy«ophenol
2.4-OlllEmLPHEMQL
BENZOIC ACID
SlKZ-CHlOKOEnaiTMCTWUIC
2,4-OICHLOROPKENOL
1,2,4-TRrCHLOROMNIEME
NAPHTHALENE
4-CHLOROMHLINE
MEXACMLOROBlfTADlENE
4-CHLORO-M-CRESOL
2-METinrUUMfNU£i(E
HEX*au.«ocTaopaT*ojE«
2,4,6-TRICW.QROPHEIIOL
2,4IS*»1CHL0RWNCML
2-CXUKOHAPHTHALENE
2-N1TMANIUNE
DlWTim. PHTRAIATE
ACEMMTNYLEME
2, 6*01H1TROTOLUENS
J-NITtOANiLINE
ACEMMTNENE
2,4-oinitropnenol
4-NITROPHENOL
oiiazoruuui
2,4-DINITROTOLUENE
DIETHYL PNTMUTE
4-CHL0R0PMI(n-PHENYLETHER
FlUQUNE
4-NITRQAMILINE
4, 6*01 N1ISO-2-METHTLPNENOL
N-NtTROSOBIPHENTUIIHlE
t-8MN0PKEKYl.-PHEIITl.ETHE*
HEXAGNLOROBENZEME
PENTACHLQROPHEHOL
PHEMNTHRENE
ANTHRACENE
OI-N-BUTYL PHTHALATE
FLUOHANTHENE
PTREKE
BUm BENZYL PHTHALATE
3,3'*OICNLQRQiaaiDllE
BEN20(A)AH(WtACEIiE
CKRYSEHE
SlS(2-ETHYlitEXYl>PHTHAUTI
DI*N*OCTYL PHTHAUTE
3EN20(t)FLlOUUITHEVZ
BENMdOriUQRAMTHENE
BEXZQMIPVREHE
IN0EN0(1,2,J,-CD)PYRENi
D18ENZ(A,H)ANTHRACEME
SEIQ9CCN1 )PERYLENE
MM
08«
F1206
H7W
11209
J21I
K411
14A07
L513
H14A08
¦(660)
•(660)
mm*
•(MO)
*0(660)
•(MO)
»(M0)
¦(660)
•(660)
10(660)
•(660)
0(660)
•(660)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
MM 660)
•(3200)
KM660)
•(3200)
•(660)
¦(660)
•(660)
•(3200)
•(660)
•(3200)
•(3200)
•(660)
•(660)
•(660)
•(3200)
N0(3200)
•(660)
•(660)
•(660)
•(1200)
•(660)
•(660)
•(660)
•(660)
•(660)
NOOSOO)
•(660)
•(660)
n a
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
NO(690)
NO(690)
NO(MO)
HD(60O)
W0(690)
K0(6m)
*0(690)
NO(«M)
•(600)
•(6M)
•(690)
ND(6W)
HO(MO)
ND(6«0)
•(690)
MKMO)
•(SUM)
•(690)
H0(6t0)
H0(«m)
ND(690)
N0(690)
*0(690)
NO (MO)
N0(6M)
NO(690)
ND(69Q)
•(MOO)
•(•m
0(3*00)
N0(6W)
•(MO)
•(610)
HO(SMO)
•(690)
•(3*00)
•(3600)
W(MO)
•(690)
•(690)
WD (MO)
•(600)
•(3*00)
•(3600)
•(6AQ)
ND(690)
HS(6M)
•(3600)
WO(690)
•(690)
52J6
•(600)
•(690)
•(600)
•(1400)
•(600)
NO(MO)
590JK
52J
•(600)
•(600)
•(690)
NO(600)
*10(600)
NS(60S)
•(620)
•(620)
•(670)
•(•70)
•(679)
•(670)
•(620)
•(670)
•(610)
•(610)
•(670)
•(670)
•(670)
•(670)
•(670)
•(3300)
•(670)
•(670)
•(670)
•(670)
•(670)
•(670)
•(670)
•(670)
•(670)
•(670)
•(3100)
•(670)
•(1300)
•(3300)
•(BOO)
•(3300)
•(3300)
•(670)
•(SSOO)
0(3300)
•(670)
•(WO)
•(*70)
•(670)
•(670)
•(3300)
•(3300)
•(670)
•(670)
•(670)
•(3300)
•(670)
•(670)
m
•(670)
•(670)
•(670)
•(1300)
0(670)
•(670)
290JB
¦(670)
•(670)
•(670)
•(670)
•(670)
•(670)
•(670)
•(660)
•(660)
ND(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
NO(660)
•(660)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(660)
ND(660)
N0(660)
N0(660)
H0(660)
•(660)
110(660)
•(660)
•(660)
•(3200)
•(660)
•(3200)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(3200)
•(3200)
•(660)
•(660)
•(660)
•(660)
•(660)
•(3200)
•(3200)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(660)
¦(660)
•(660)
•(660)
1101
•(130O)
•(660)
•(660)
200J
120J
•(660)
•1660)
•(660)
•(660)
•(660)
•(660)
•(660)
ND(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(3200)
N0(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(3200)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(3200)
•(3200)
•(660)
•(660)
•(660)
•(660)
•(660)
0(3200)
•(3200)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(660)
m
•(660)
ND{660)
•(660)
•(1300)
NO(660)
•(660)
¦(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(660)
HD(660)
ND(660)
•(660)
•(660)
•(660)
NO(660)
•(660)
•(660)
•(660)
•(660)
•(660)
•(3200)
•(660)
•(660)
•(660)
•(660)
•(660)
NO (660)
ND(660)
•(660)
•(660)
N0(660)
•(38)0)
N0(660)
•(3200)
•(660)
N0(660)
•(660)
•(3200)
•(660)
•(3200)
•(3200)
NO(660)
NO(660)
604
ND(660)
•(660)
NOI3200)
•(3200)
N0(660)
•(660)
•(660)
•(3200)
•(660)
•(660)
2400*
•(660)
ND(660)
•(660)
0(1300)
•(660)
NO(660)
650JB
N0(660)
•(660)
N0(660)
N0(660)
KD(660)
•(660)
•(660)
WD(670)
N0(670)
NB(670)
•(670)
•(670)
•(670)
•(670)
NO(670)
•(670)
N0(670)
N0(670)
•(670)
N0(67D)
ND(670)
•(670)
N0(670)
•(3200)
N0(670)
WO(670)
•(670)
ND(670)
NDC670)
•(670)
WO(670)
•(670)
•(670)
ND(670)
WO(3200)
•(670)
•(3200)
N0(670)
•(670)
•(670)
•(3200)
•(670)
•(3200)
N0(3200)
NO(67Q)
•(670)
¦(670)
•(670)
•(670)
•(3200)
•(3200)
N0(670)
•(670)
•(670)
•(3200)
ND(670)
•(670)
34JO
•(670)
ND(670)
•(670)
•(1300)
WD(670)
WO (67<0)
au»
WO(670)
•(670)
ND(670)
•(670)
NO (670)
ND(670)
N0(670)
•(660)
HO(660)
N0(660)
HO(660)
•(660)
HO (660)
HO(660)
•(660)
ND(660)
HB(660)
H0(660)
•(660)
•(660)
•(660)
NO(660)
•(660)
ND(3200)
ND(660)
HO(660)
HD(660)
H0(66O)
N0(660)
HO(660)
WO(660)
N0(660)
ND(660)
WO(660)
•(3200)
•(660)
•(3200)
•(660)
HO(660)
•(660)
•(3200)
NO(660)
•(3200)
•(3200)
ND(660)
N0(660)
NO(660)
•(660)
•(660)
WO(J200>
NO(3200)
•(660)
N0(660)
•(660)
•(3200)
•(660)
•(660)
380J
W0(66O)
H0(66O)
NO(660)
•(1300)
H0(660)
N0(660)
150J1
•(660)
•(660)
•(660)
N0(660)
•(660)
N0(660)
•(660)
N0(680)
N0(660)
•(660)
•(600)
•(680)
NO(680)
N0(680)
WD(660)
•(680)
•(680)
N0(680)
NO(680)
ND(680)
N0(680)
NO(680)
NO(680)
•(3300)
NS(680)
NS(680)
•(680)
NS(680)
NS(680)
•(660)
N0(680)
•(680)
•(680)
ND(680)
•(3300)
H0(680)
•(3300)
N0(680)
H0(680)
•(680)
•($300)
•(680)
•(3300)
•(600)
NOC600)
•(680)
•(680)
NSC680)
NO(680)
•(3300)
N0(3300)
N0(680)
•(680)
W0(6M)
NO(3300)
HO(680)
•(680)
¦(680)
•(680)
ND(680)
WS(680)
•(1400)
•(680)
N0(660)
660JS
•(680)
N0(680)
ND(680)
NO(680)
NO(680)
•(680)
•(660)
NO(660)
•(660)
HO(660)
•(660)
•(660)
H0C66O)
•(660)
•(660)
•(660)
N0(660)
•(660)
•(660)
10(660)
•(660)
•(660)
ND(660)
i0(3200)
•(660)
N0(660)
ND(660)
N0(660)
HO(660)
W0(660)
N0(660)
WO(660)
N0(660)
•(660)
•(3200)
WD(3200)
•(660)
•(660)
ND(660)
WO(660)
•(3200)
•(660)
•(3200)
ND(3200)
•(660)
•(660)
•(660)
•(660)
•(660)
•(3200)
N0CI200)
•(660)
N0(660)
•(660)
•(3200)
180J
66J
110 i
3604
3801
•(660)
•(13001
ISO!
MOI
160A
•(660)
6001
W0(660)
220J
190J
WD(660)
280i
ALL ANALYTICAL RESULTS EXPRESSED AS IK/SO.
•(660) ¦ COMPOUND NOT DETECTED WIN DETECTION LIMIT IK PARENTHESES
S ¦ AHALVTE FOUND IN THE ASSOCIATES SUUK AS UEU. AS THE SAMPU
i ¦ ESTIMATES VALUE - RESULT IS LESS THAN THE OUAMTIHCATtON LIMIT SUT GREATER THAN ZERO
TTLC (TOTAL TWRSKU LIMIT CORCSmUTION) VALUES MM CALIFORNIA ADMINISTRATIVE CODE, TITLE 22, SECTION 66*99.
H.A. • TTLC HOT AVAILABLE
17

-------
TABLE 2. (Continued)
compouw
HUM
*510
nrfftTI nw
Nil*
iawus
P71»
pan
Rt«ir
OEIMO
SAMPLE
0701
CALIFORNIA
mc
tug/kg)
PHQtt.
•(680)
NO(MO)
•(6tt)
•(660)
•(670)
•(670)
•(670)
N.A.
3IS(2-CHLORO£TKTL)ETt®l
•(680)
•(600)
W(6M)
•(660)
•(670)
•(670)
•(670)
N.A.
2-CHLCROPHENOL
•(680)
•(600)
ND(660)
•(MO)
•(•ID)
•(670)
•(670)
H.A.
1,3-DICXlOftOKKENS
•(MO)
•(MO)
•(660)
•(MO)
•(670)
•(MO)
•(670)
N.A.
i,t»piaaoBnw«rm»
•(680)
NO(MO)
•(660)
•(MO)
•(670)
•(670)
•(*70)
N.A.
8EKZTL ALCOHOL
10(680)
•(690)
•(6M)
W(6M)
•(ATS)
•(670)
•(*70)
N.A,
1, >¦«»"' Moimin
NKMO)
•(600)
•(MO)
•(660)
•(AID)
•(670)
•(670)
N.A.
2-NcmuMawiL
•(AM)
•(*90)
•(660)
•(MO)
•(AID)
•(670)
•(670)
K.A.
s i ta-cmaeat soptopn iethei
•(680)
K0(690)
•(MO)
W(6M)
•(AID)
•(670)
•(*70)
N.A.
4-NeTKTLPHENOL
•MM)
HO(MO)
•(MO)
•(MO)
•(670)
•(670)
•(470)
M.A.
K-NITtOSODl-N-PtOPTLAMIM
•(680)
•(MO)
•(6»)
•(6M)
•(670)
•(670)
•(670)
N.A.
HEXAOU.OSQCTHANS
•(400)
•(600)
•(660)
•(660)
•(670)
•(670)
•(470)
M.A.
*iiK»eiizEi«
•(MO)
NO(MO)
•(660)
•(MO)
•(670)
•(670)
•(470)
M.A.
ISOMKONI
•IMS)
•(690)
•(6M)
•(660)
•(MO)
•(670)
•M70)
N.A.
2-NlTtGPMEWS.
•(680)
•(MO)
NO(660)
•(660)
•(670)
•(670)
•(470)
M.A.
2,4-OIWTKTl.PfiENOt.
•(MO)
ND(MO)
•(660)
•(660)
•(670)
•(A78)
•(470)
K.A*
BENZOIC ACID
•(3300)
•(3400)
•(3200)
•(3200)
•(3200)
•(3300)
•(3300)
N.A.
8is(Z-CKLQRainncTweTMUii
•(680)
KMMO)
•(660)
•(MO)
•(AID)
•(670)
•1*70)
K.A.
2,4-OICHUKOraEHOL
•(MO)
•(MO)
•(660)
•(660)
•(478)
•(670)
•(470)
N.A.
1,2,4-TRICHLOOMMEa
•(MO)
•(MO)
•(660)
•(MO)
•(670)
•(670)
•(470)
K.A.
NAMTMLfNE
W(MO)
•(690)
W(6M)
•(660)
M(470)
•(610)
•(470)
N.A.
4-CHiatOMlLIIIE
W(MO)
•(M8>
•(600)
•(660)
•(AM)
•(670)
•(670)
•(*70)
K.A.
XEXACNLOROBffABItW
NO(MO)
•(660)
•(AM)
•(MO)
•(670)
•(470)
N.A.
4-CHLOKO-H-CtESOL
•(MO)
ND(tfO)
•(660)
•(660)
•(670)
•(670)
•(470)
N.A.
2'NHmWMTMUIIC
W(MO)
•(690)
•(660)
•(660)
•(670)
•(MO)
•(470)
N.A.
HEwmwocraopatTtttCKE
•(680)
NSMOO)
•(*60)
•(660)
•(670)
•(670)
•(470)
N.A.
2,4,6-TRICHlORyWMH
•(MO)
HS(MO)
W(6M)
•(6M)
•(MO)
•(670)
•(470)
N.A.
2,4,S*TWCHU*8»NHI0l
•(S300)
110(3400)
•(3200)
•(3200)
•(3200)
•(3300)
•(3300)
N.A.
2-CH10B0NAFNTIMLENE
•(MO)
NO(MO)
•(660)
•(660)
•(670)
•(670)
•(470)
N.A.
2-nitkkuiiljhe
•(3300)
•(3400)
•(3200)
•(3200)
•(3200)
•(1300)
•(3300)
N.A.
OIWTHTL PHTHALATE
•(MO)
•(600)
•(660)
•(AM)
ND(MO)
•(670)
•(*70)
N.A.
ACEWPNTHTLEUE
•(MO)
•(AOO)
•(660)
•(6M)
•(670)
•(670)
•(670)
K.A.
2,6-OINITROTOLUEIIE
•(MO)
*0(690)
N0(6M)
•(AM)
•(670)
•(670)
•(470)
N.A.
J-NITtOANUUE
•(3300)
•(3400)
•(3200)
•(3200)
•(3200)
•(3300)
•(3300)
N.A.
ACtMMTMENt
mm)
•(690)
•(6M)
•(660)
•(MO)
•(670)
•(470)
N.A.
2,4-ouiTRCPMNa
•(3300)
•(3400)
•(3200)
•(3200)
•(3200)
•(3300)
•(3300)
N.A.
(•Humnot.
•(3300)
•(3(00)
•(3200)
•(3200)
•(3200)
•(3300)
•(3300)
N.A.
oiisuruRM
•(MO)
•(MO)
•(6M)
•(AM)
•(•10)
•(*70)
•(470)
N.A.
2,4*INITROTOLU«ff
KMMO)
•(MO)
•(660)
•(AM)
•(670)
•(670)
•(470)
N.A.
DIETITl. PHTHALATE
man
•(600)
•(660)
•(AM)
•(MQ)
•(670)
•(*70)
N.A.
4-CKLONOPKENYl-PHENTLETHO
HO(MO)
W(MO)
•(6M)
•(AM)
•(670)
•(670)
•(*70)
M*A«
FlUQUNE
•(MO)
•MOO)
ND(660)
•(AM)
•(670)
•(670)
•(*70)
N.A.
4-NIT10AN1LIU
•(3300)
•(3400)
•(3200)
•(3200)
•(3200)
•(3300)
•(S300)
N.A.
4,6-0l»IT*O-2-«IHTlPKE)(01
•(3300)
•(3400)
•(3200)
•(3200)
•(3200)
•(3300)
•(1300)
N.A.
N-NITBOSODlMtENYUUIIIII
•(MS)
ND(600)
•(660)
•(660)
• (670)
•(670)
•(*70)
N.A.
4-aeaa>*E*TL-pnenuethei
•(480)
•(600)
•(660)
•(AM)
•(*70)
•(670)
•(470)
N.A.
HEXACMLOCOBENZEME
•(MO)
ND(600)
ND(6M)
•(AM)
•(670)
•(670)
•(470)
N.A.
PENTACXLOEOPKENOL
H(SSOO)
•(3400)
•(3200)
•(3200)
•(3200)
•(3300)
•(3300)
17000
PKENANTHRME
•(660)
•(600)
W(6M)
•(AM)
•(670)
•(670)
•(470)
N.A.
ANTWACENE
•(MO)
•(600)
•(660)
•(AM)
*0(670)
•(670)
•(470)
N.A.
Ol-N-«UfTl PKTKALAfE
62J
10M W(660)
•(AM)
8SJ •(670)
•(670)
N.A.
FLUOtANTKENE
•(MO)
•(600)
•(660)
•(660)
73J 10(670)
•(670)
N.A.
PME»E
•(680)
•(600)
•(660)
•(AM)
9ij mum
•(670)
N.A.
aurn bemztl phtkalate
W(MO)
•(600)
•(660)
•(MQ)
200J W(670)
•(470)
N.A.
J.S'-OIOCUXOBEIBIOINE
•(1400)
•(1400)
•(1300)
0(1300)
•(1300)
•(1300)
•(1300)
N.A.
3£UO(A)ANTHIACENE
•(MO)
•(*90)
•(660)
•(AM)
•(678)
•(670)
•(MO)
N.A.
CHRTSEME
W(MO)
•(600)
•MM)
•(AM)
•(MO)
•(670)
•(470) •
N.A.
BIS(2-EI KrLKEXTL )PHTKALATE
130JS
620JB
120J
BUS
130MB
1001
240JI
N.A.
DI-II-OCTU PHTNAUTE
•(MO)
MO(690)
•(6M)
•(AM)
49J
•(670)
•(470)
N.A.
BSBOttJFUJOtANTNENi
W(MO)
•(690)
•(660)
•(AM)
•(670)
•(670)
•(470)
N.A.
BE«D(K)FLUOM«tHEttE
•(660)
•(600)
•(660)
•(AM)
ND(A70)
•(670)
•(670)
N.A.
8E*20(A)mEW
•(480)
W(MO)
W(6M)
•(6M)
•(670)
•(670)
•(670)
N.A.
IWEN0(1,2,3,-C0)PYRENt
•(680)
•(600)
•(660)
•(AM)
N0(670)
•(670)
•(670)
N.A.
DIBBa(A,H)ANTN*ACENE
•(660)
•(600)
•(6M)
W(6M)
•(670)
•(670)
•(670)
N.A.
lENMGHI)PERYLE*E
•(MO)
•(690)
MD(6dO)
•(AM)
N0(670)
•(670)
•(670)
N.A.
18

-------
TABLE 3. SUMMARY OF SOIL ANALYSIS RESULTS FOR PESTICIDE COMPOUNDS
MeFARLAND, CALIFORNIA
COMPOUND
0414
080Z
F1204
*709
BHC-ALPHA
NDO60)
*0(168)
*D(163)
*0(160)
BHC-IETA
ND(160)
*0(168)
*0(163)
*0(160)
BHC'OELTA
NDO60)
*0(168)
*0(163)
*0(160)
BHC'GAMMA (LINDANE)
ND(160)
N0(168)
ND(163)
ND(IAO)
HEPTACHLOR
ND(160)
*0(168)
*0(163)
*0(160)
ALORIN
ND(160)
ND(168)
N0(163)
N0(160)
HEPTACHLOR EPOXIOE
ND(160)
*0(168)
*0(163)
*0(160)
ENDOSULFAN 1 (ALPHA)
ND(160)
*0(168)
N0(163)
*0(160)
OIELDRIN
ND(320)
*0(336)
*0(327)
*0(320)
4,4'*0DE
ND(320)
*D(336)
*0(327)
*0(320)
ENORIN
ND(320)
*0(336)
N0(327)
NO (320)
ENDOSULFAN 2 (BETA)
ND(320)
N0(336)
N0(327)
NO(320)
4,4'«D0D
N0(320)
*0(336)
N0(327)
NO(320)
ENDOSULFAN SULFATE
ND(320)
*0(336)
*0(327)
NO(320)
4,4'*D0T
*0(320)
*0(336)
*0(327)
*0(320)
NETNOKYCHLOR
*0(1602)
*0(1682)
*0(1633)
ND(1602)
ENORIN KETONE
ND(320)
*0(336)
N0(327)
*0(320)
CHLORDANE, ALPHA
ND(160)
N0(168)
*0(163)
*0(160)
CHLORDANE .BETA
N0(160)
*0(168)
*0(163)
*0(160)
TOXAPNENE
ND(3203)
*0(3365)
*0(3265)
NO(3203)
PC8-1016 (AROCLOR 1016)
*0(1602)
*0(1682)
*0(1633)
NO(1602)
PCS*1221 (AROCLOR 1221)
*0(1602)
ND(16B2)
ND(1633)
N0(1602)
PCS-1232 (AROCLOR 1232)
*0(1602)
*0(1682)
*0(1613)
*0(1602)
PCS-1242 (AROCLOR 1242)
*0(1602)
*0(1682)
*0(1633)
ND(1602)
PCB-1Z4A (AROCLOR 124S)
*0(1602)
*0(1682)
*0(1633)
N0(1602)
PCB-12S4 (AROCLOR 1234)
*0(3203)
*0(336S)
N0(326S)
*0(3203)
PCS-1260 (AROCLOR 1260)
*0(3203)
*0(3363)
*0(3265)
NO(3203)
NcMUANO SAMPLES
11209
¦1212
K411
L4A07
NO(160)
*0(160)
*0(160)
*0(160)
ND(160)
*0(160)
ND(160)
*0(160)
ND(160)
ND(160)
ND(160)
*0(160)
*0(160)
*0(160)
ND(160)
ND(160)
N0(160)
*0(160)
*0(160)
*0(160)
*0(160)
*0(160)
NO(160)
N0(160)
N0(320)
N0(321)
*0(320)
1057
*0(321)
NO(320)
NO(320)
N0(321)
*0(320)
*0(320)
*0(321)
*0(320)
N0(320)
N0(321)
*0(320)
*0(320)
*0(321)
*0(320)
*0(320)
*0(321)
*0(320)
N0(1600)
N0(1603)
N0(1600)
*0(320)
*0(321)
*0(320)
N0(160)
*0(160)
NO(160)
*0(160)
*0(160)
*0(160)
N0(3200)
N0(3206)
N0(3200)
*0(1600)
*0(1603)
*0(1600)
ND(1600)
ND(1603)
N0(1600)
*0(1600)
*0(1603)
*0(1600)
N0(1600)
N0(16Q3)
N0(1600)
*0(1600)
*0(1603)
*0(1600)
N0(3200)
N0(3206)
ND(3200)
*0(3200)
*0(3206)
*0(3200) !
L5ts
HUMS
NO(160)
N0(160)
N0(160)
ND(160)
N0(160)
N0(160)
*0(160)
*0(160)
*0(320)
*0(320)
NO(320)
NO(320)
*0(320)
NO(320)
NO(320)
*0(1600)
NO(320)
*0(160)
N0(160)
ND(3200)
HOC1600)
*0(1600)
*0(1600)
*0(1600)
*0(1600)
NO(3200)
*0(3200)
*0(164)
*0(164)
*0(164)
*0(164)
*0(164)
*0(164)
*0(164)
*0(164)
*0(328)
*0(328)
*0(328)
*0(328)
*0(328)
*0(328)
*0(328)
*0(1639)
*0(328)
N0(164)
*0(164)
*0(3279)
*0(1639)
N0(1A39)
*0(1639)
N0(1639)
*0(1639)
*0(3279)
*0(3279)
N0(161)
*0(161)
ND(161)
*0(161)
ND(161)
*0(161)
N0(1«1)
*0(161)
*0(321)
N0(321)
*0(321)
*0(321)
N0(321)
*0(321)
N0(321)
*0(1606)
N0(321)
*0(161)
N0(161)
*0(3213)
N0(1606)
*0(1606)
N0C1606)
*0(1606)
*0(1606)
*0(3213)
UK3213)
ALL ANALYTICAL RESULTS EXPRESSED AS UG/KC.
*0(660) ¦ COMPOUND NOT DETECTED UITH DETECTION LIMIT IN PAUNTHZSES
B ¦ ANALVTE FOUND IN THE ASSOCIATED IUUUC AS (JELL AS THE SAMPLE
J * ESTIMATED VALUE • RESULT IS LESS THAN THE QUANTIFICATION LIMIT BUT GREATER THAN ZERO
TTLC (TOTAL THRENOLO LIMIT CONCENTRATION) VALUES FRGN CALIFORNIA ADMINISTRATIVE CODE, TITLE 22, SECTION 66699.
N.A. ¦ TTLC and ITLC NOT AVAILABLE
19

-------
TABLE 3. (Continued)
OELANO CALIFORNIA
NcMKLANO SAMPLES	SAMPLE	TTLC
COMPOUND
NM06
MS10
M116
P71S
P8CB
R1417
0F01
(ug/kg)
BHC-ALPHA
ND(166)
ND(168)
ND(160)
ND(161)
*0(163)

ND(B2)
N.A.
BHC-BETA
ND(166)
ND(168)
N0(160)
N0(161)
NO(163)

ND(B2)
N.A.
BHC-OELTA
ND(166)
ND(168)
ND(160)
ND(161)
ND(163)

N0(82)
N.A.
BHC-CAMW (LINDANE)
ND(166)
N0(168)
ND(160)
*0(161)
*0(163)

N0(B2)
4000
HEPTACHLCR
N0(166)
ND(168)
ND(160)
ND(161)
ND(163)

ND(B2)
4700
ALORIN
ND(166)
ND(168)
ND(160)
N0(161)
*0(163)

N0(B2)
1400
HEPTACHLOR EPOXIDE
NO(166)
ND(168)
ND(160)
ND(ldl)
ND(16I)
SAIVLE
ND(82)
N.A.
ENDOSULFAN 1 (ALPHA)
N0(166)
N0(168)
KD(160)
N0C161)
*0(163)

ND(B2)
N.A.
DIELORIN
N0(331)
ND(336)
ND(321)
NO(322)
ND(326)

N0(163)
8000
4.V-00E
N0(331)
*0(336)
N0(321)
ND(322)
*0(326)

ND(163)
1000
ENOIIN
ND(331)
*0(336)
ND(321)
ND(322)
*0(326)

ND(163)
200
ENDOSULFAN 2 (BETA)
ND(331)
N0(336)
ND(321)
N0(322)
HD(326)

NO (163)
N.A.
4,4'-0DD
N0(33t)
*0(336)
*0(321)
ND(322)
*0(326)

*0(163)
1000
ENDOSULFAN SULFATE
ND(331)
*D(336)
ND(321)
*0(322)
ND(326)
NOT
*0(163)
N.A.
4,4'-00T
ND(331)
N0(336)
ND(321)
N0(322)
*0(326)

ND(163)
1000
METHOXTCHLOR
NO(1656)
ND(14B2)
NO(1603)
ND(1611)
ND(1628)

ND(815)
100000
ENORIN KETONE
ND(331)
*0(336)
ND(321)
ND(322)
*0(326)

ND(163)
N.A.
CHLORDANE,ALPHA
N0(166)
ND(168)
ND(160)
ND(161)
ND(16I)

ND(82)
2500
CHLORDANE,BETA
NO (166)
ND(t68)
*0(160)
*0(161)
*0(163)

ND(82)
2500
TOXAPHENE
ND(3313)
*0(3365)
ND(3206)
N0(3223)
ND(3235)

ND(1631)
sooo
PCR-1016 (AROCLOR 1016)
ND(1656)
ND(1682)
ND(1603)
ND(1611)
N0(1628)
ANALYZED
*D(815)
soooo
PCS-1221 (AROCLOR 1221)
*0(1656)
ND(1682)
*0(1603)
*0(1611)
*0(1623)

ND(815)
50000
PCB-123Z (AROCLOR 1232)
ND(1656)
ND(1682)
ND(1603)
ND(1611)
NO(1622)

ND(815)
soooo
PCI-1242 (AROCLOR 1242)
N0(16S6)
ND(1682)
NO(1603)
N0(1611)
*D(1623)

ND(81S)
soooo
PCS*1248 (AROCLOR 1248)
WO(1636)
*0(1662)
N0(1A03)
*0(1611)
*0(1623)

ND(81S)
soooo
PCBMZ54 (AROCLOR 12S4)
N0(3313)
*D(3365)
N0(3206)
N0(3223)
*0(3255)

ND(1631)
soooo
PCB-1260 (AROCLOR 1260)
ND(3313)
*D(3365)
N0(3206)
N0(3223)
N0(3235)

ND(1631)
soooo
20

-------
TABLE 4. CURSORY STATISTICAL ANALYSIS FOR SOIL SAMPLING
METAL RESULTS, McFARLAND, CA
Samples #
n-1
3SD
X+3SD
Aluminum 17
159,280
9,369
3,238
9.714
19,083
Antimony 17
210
12.4
0.71
2.13
14.53
Arsenic 17
316
18.5
60.7
182.1
200.6
Barium 17
1,907
112.1
37.2
111.6
223.7
Beryllium 17
7.18
0.42
0.18
0.54
0.96
Cadmium 17
16.68
0.98
0.40
1.20
2.18
Calcium 17
65,970
3,880
1,512
4,536
8,416
Chromium 17
295
17.3
5.86
17.58
34.88
Cobalt 17
137
8.10
2.76
8.28
16.38
Copper 17
560
32.9
77.1
231.3
264.2
Iron 17
232,100
13,652
5,462
16,386
30,038
Lead 17
647
38.1
55.6
166.8
204.9
Magnesium 17
68,480
4,028
1,455
4,365
8,393
Manganese 17
4,535
266
75
225
491
Mercury 17
5.78
0.34
0.46
1.38
1.72
Nickel 17
248.9
14.6
6.2
18.6
33.2
Potassium 17
65,750
3,867
1,260
3,780
7,647
Selenium 17
*
*
*
*
*
Silver 17
21.9
1.28
0.40
1.2
2.48
Sodium 17
7,942
467
111
333
800
Thallium 17
7.9
0.46
0.21
0.63
1.09
Vanadium 17
548
32.2
10.6
31.8
64.0
Zinc 17
1,491
87.7
106
318
405.7
*Not calculated
- metal not detected.



21

-------
TABLE 5. CURSORY STATISTICAL ANALYSIS FOR SOIL SAMPLING
METAL RESULTS, MINUS OUTLIERS, McFARLAND, CA

Samples #
h
X

3SD
X+3SD
Arsenic
16
62.1
3.8
3.29
9.87
13.67
Cadmium
16
14.48
0.90
0.25
0.75
1.65
Copper
16
228
14.2
4.7
14.1
28.3
Lead
16
425
26.6
30.1
90.3
111.9
Mercury
16
3.98
0.24
0.28
0.84
1.08
Vanadium
16
483.5
30.2
6.93
20.79
50.99
Zinc
16
1,014
63.3
36.67
110.01
173.31
22

-------
McFarland
Study Area
*9, 1989
V'3885'
Ltigend—
itudv Area
(oumrlary
Browning
i	<
Ccipol
» *-"* er*w V f Vi iCTK ' I
'XV' !> i . ¦ %SS % • '.£
!iF®aB6i qkt ;i
*	.,«; 5 no.
uwumi- sws&s


-------
Appendix 1
X-RAY FLUORESCENCE SCREENING SURVEY
McFarland, California
A1

-------
CONTENTS
Information and Regional Request	Sheet A
Data Quality Objective Summary	Sheet B
Principles of XRF and Instrument Specifications	Sheet C
Quality Control and Calibration	Sheet D
XRF Survey Data	Sheet	E

-------
Sheet A
Information and Regional Request
EPA Region: IX	Regional Science Advisor: Arnold Den
Regional OSC: Matthew Monsees
EMSL Project Officer: Ken Scarbrough
Site Name: McFarland, CA
Site Protection Level: No protective gear required
Time Frame: from July 18 - 20, 1989
EPA on-site Contractors: Ecology and Environment; Lockheed ESC
Elements sought: Arsenic (As), Lead (Pb), Chromium (Cr),
Description of Work Requested: Systematic XRF screening of soils
over the entire townsite, to determine the relative ranges of
potential toxic metal contamination.

-------
Sheet B
Data Quality Objective Summary Form
1. Site: McFarland, CA	EPA Region: IX
2. Sample Media: soil
3. Data Use: site screening
4. Description of Work Requested: systematic screening of soils
over the townsite on a regular grid to characterize potential
toxic metal contamination levels in a relative sense.
5. Site Information:
Area: Townsite	Depth to ground water: Unknown
Ground water use: Irrigation and possibly drinking water
Soil Types: See soil sampling report data
Sensitive Receptors: Local residents
6. Sampling Method to be Used:
Non-intrusive, grid sampling
7. Sampling procedures:
For FPXRF field screening, three measurements are taken at
each sampling point, in a small triangular pattern. Three
measurements are taken to reduce the sampling variability and
to obtain a more representative sample.

-------
Sheet C
PRINCIPLES OF X-RAY FLUORESCENCE
X-ray fluorescence (XRF) is based on the principle that photons
produced from an X-ray tube or radioactive source bombard the
sample to produce fluorescence. The incident photons impinge on
the electron cloud of the atom. Among other events, this process
creates vacancies in one or more of the inner shells. The
vacancies cause instability within the atom. As the outer
electrons seek stability by filling the vacancies in the inner
shells, the atom emits energies as X-ray photons. The emitted
energy (fluorescence) from a particular shell is characteristic of
the atom in which it was produced and is equal to the difference in
bonding energy between the outer shell electron and the vacant
shell. Most elements under the photon bombardment fluoresce
simultaneously to produce a spectrum of characteristic radiation.
It is this spectrum that the detector senses and counts.
There are two types of XRF spectrometers, energy dispersive and
wavelength dispersive. The principal differences are in the method
of detection of the fluorescent energies of the specimen and the
method of quantifying the analytes of interest. The field portable
XRF instrument used in this program is an energy dispersive
spectrometer.
The X-MET 880:
Field Portable X-ray Fluorescence Spectrometer
The X-Met 880 is a field portable, energy dispersive X-ray
fluorescence spectrometer marketed by Columbia Scientific
Industries Corporation, Austin, TX. The unit is self-contained,
battery powered, microprocessor based and weighs 8.5 kg. The
surface analysis probe is specifically designed for field use. The
X-Met 880 is hermetically sealed and can be decontaminated with
soap and water. The probe includes a radioisotope source of
Curium-244, a proportional counter and the associated electronics.
The source is protected by an NRC-approved safety shutter.
The electronic unit has thirty-two calibration memories called
•models'. Each model can be independently calibrated for as many
as six elements. These can be used to measure elements from
silicon to uranium assuming the proper isotope source is available.
The unknown sample intensities are regressed against the
calibration curves to yield concentrations.

-------
Sheet D
Quality Control for
Screening In Situ
Quality Control
For any method of instrumental chemical analysis that utilizes
a calibration curve, the physical composition of the calibration
standards must be closely matched to the physical composition of
the samples for routine analysis (i.e., the matrices must match).
Once an instrument is calibrated and routine analysis proceeds, the
instrument must be periodically checked for stability (base line
drift and gain change) . Base line drift is monitored by
periodically running zero- or near zero-concentration check
samples. Gain change is monitored by periodically running mid-
calibration range check samples. These check samples must also
closely match the matrices of the calibration standards and the
routine samples. The low concentration check sample is used to
determine the detection limits and the mid-calibration range sample
is used to determine accuracy. Precision is generally determined
on split (or duplicate) samples.
At McFarland, 2 X-Met 880s were used. One instrument was
calibrated during a training session at the manufacturer's
facilities and the other by the Region 6 team from which the
instrument was borrowed. The calibration curves were based on a
spiked soil; the matrix of which is distinctly different from that
of the soils at McFarland. For this reason the data can not be
considered quantitative.
Bias between the two instruments was not investigated so it
was decided that each instrument would be used on only one side of
the highway dividing McFarland to avoid data comparability issues
(i.e., instrument A was to remain on the east side and instrument
B on the west side). To avoid the data comparability issue, two
distinct populations of data were created. This, combined with the
fact that the data is non-quantitative, is our rationale for not
attempting to contour or interpret the data. The data for each
instrument are plotted separately on the attached figures.
QA considerations require that both teams employ identical
standards for continuing instrument stability checks. There was
only one set of standards available and no duplicates in the set so
each team used different mid-calibration range check standards.
Detection limits could not be determined because of matrix
differences between the low level check samples and the local soil.

-------
Sheet E
FPXRF Survey Data
The sample values in this raw data table are unitless instrument
readings.
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
McFarland Grid Points
SAMPLE ID
Cr
As
Pb
01A
0.009
0.022
0.000
01B
0.135
0.000
0.000
01C
0.162
0.000
0.000
01D
0.198
0.003
0.017
01E
0.181
0.000
0.000
OIF
0.194
0.000
0.000
01G
0.129
0.000
0.000
01H
0.152
0.000
0.000
Oil
0.253
0.000
0.000
01J
n.S.
n.s.
n.s.
OIK
n.s.
n.s.
n.s.
OIL
n.s.
n.s.
n.s.
01M
n.s.
n.s.
n.s.
01N
n.s.
n.s.
n.s.
02A
0.032
0.007
0.001
02B
n.s.
n.s.
n.s.
02C
n.s.
n.s.
n.s.
02D
n.s.
n.s.
n.s.
02E
0.194
0.000
0.000
02F
0.157
0.000
0.000
02G
0.181
0.000
0.000
02H
0.246
0.000
0.000
021
0.152
0.000
0.000
02J
n.s.
n.s.
n.s.
02K
n.s.
n.s.
n.s.
02L
n.s.
n.s.
n.s.
02M
n.s.
n.s.
n.s.
02N
n.s.
n.s.
n.s.
03A
0.024
0.014
0.000
03B
n.s.
n.s.
n.s.
03C
n.s.
n.s.
n.s.
03D
n.s.
n.s.
n.s.
03E
0.121
0.000
0.000
03F
0.159
0.000
0.000
03G
0.186
0.000
0.000
03H
0.186
0.000
0.000
031
0.151
0.025
0.095
03J
n.s.
n.s.
n.s.
03K
n.s.
n.s.
n.s.

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
SAMPLE ID
cr
As
Pb
03L
n.s.
n.s.
n.s.
03M
n.s.
n.s.
n.s.
03N
n.s.
n.s.
n.s.
04A
0.027
0.023
0.000
04B
n.s.
n.s.
n.s.
04C
n.s.
n.s.
n.s.
04D
n.s.
n.s.
n.s.
04E
0.175
0.001
0.000
04F
0.187
0.000
0.000
04G
0.149
0.000
0.000
04H
0.239
0.000
0.000
041
0.122
0.000
0.000
04 J
n.s.
n.s.
n.s.
04K
n.s.
n.s.
n.s.
04L
0.062
0.016
0.000
04M
0.018
0.020
0.000
04N
0.021
0.012
0.000
05A
0.053
0.027
0.000
05B
n.s.
n.s.
n.s.
05C
n.s.
n.s.
n.s.
05D
n.s.
n.s.
n.s.
05E
0.226
0.000
0.000
05F
0.148
0.000
0.000
05G
n.s.
n.s.
n.s.
05H
0.165
0.000
0.000
051
0.130
0.000
0.000
05J
n.s.
n.s.
n.s.
05K
0.049
0.071
0.000
05L
0.071
0.010
0.000
05M
0.023
0.018
0.000
05N
0.054
0.014
0.000
050
0.048
0.018
0.000
05P
0.041
0.015
0.000
06A
0.033
0.017
0.000
06B
n.s.
n.s.
n.s.
06C
n.s.
n.s.
n.s.
06D
n.s.
n.s.
n.s.
06E
n.s.
n.s.
n.s.
06F
n.s.
n.s.
n.s.
066
n.s.
n.s.
n * s •
06H
0.18 6
0.000
0.000
061
0.167
0.000
0.000
06 J
n.s.
n.s.
n.s.
06K
0.031
0.019
0.000
06L
0.022
0.016
0.000

-------
(Note: n.s. « not sampled due
to inaccessibility or lack of
permission)
SAMPLE ID
06M
06N
060
06P
07A
07B
07C
07D
07E
07F
07G
07H
071
07J
07K
07L
07M
07N
070
07F
08A
08B
08C
08D
08E
08F
08G
08H
081
08J
08K
08L
08M
08N
080
08P
08Q
08R
08S
08T
08U
09A
09B
Cr
0.026
n.s.
0.050
0.040
0.063
n.s.
n.s.
n.s.
n.s.
n.s.
n.s.
0.120
0.199
n.s.
0.042
0.050
0.074
n.s.
0.047
0.017
0.034
n.s.
0.209
0.160
0.183
0.138
0.195
0.180
0.152
n.s.
0.042
0.025
0.002
0.033
0.018
0.037
0.046
0.028
0.016
n.s.
n.s.
0.035
n.s.
As
0.008
n.s.
0.013
0.018
0.009
n.s.
n.s.
n.s.
n.s.
n.s.
n.s.
0.000
0.000
n.s.
0.020
0.014
0.015
n.s.
0.018
0.016
0.022
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
0.021
0.016
0.015
0. 014
0.009
0.013
0.016
0.015
0.017
n.s.
n.s.
0.014
n.s.
Pb
0.001
n.s.
0.000
0.000
0.012
n.s.
n.s.
n.s.
n.s.
n.s.
n.s.
0.000
0.000
n* S •
0.000
0.000
0.017
n.s.
0.000
0.000
0.005
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
net
• s •
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
n.s.
0.000
n.s.

-------
(Note: m. = not sampled due
to inaccessibility or lack of
permission)
SAMPLE ID
09C
09D
09E
09F
09G
09H
091
09J
09K
09L
09M
09N
090
09P
09Q
09R
09S
09T
09U
10A
10B
10C
10D
10E
10F
10G
10H
101
10 J
10K
10L
10M
ION
100
10P
10Q
10R
11A
11B
11C
11D
HE
11F
cr
0.206
0.165
0.155
0.131
0.139
0.143
0.199
0.150
0.057
0.053
0.000
0.025
0.033
0.052
0.039
0.056
n.s.
n.s.
n.s.
0.055
n.s.
0.211
0.157
0.177
0.142
0.106
0.163
0.182
0.101
n.s.
0.024
0.013
0.037
0.039
0.021
0.013
0.045
0.038
n.s.
0.194
0.152
0.145
0.208
As
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.020
0.009
0.009
0.016
0.015
0.017
0.018
0.012
n.s.
n.s.
n.s.
0.020
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
0.012
0.020
0.015
0.012
0.018
0.015
0.019
0.016
n.s.
0.000
0.000
0.000
0.000
Pb
0.000
0.000
0.000
0.000
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
n.s.
n.s.
0.000
n.s.
0.000
0.017
0.000
0.032
0.000
0.000
0.000
0.000
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
0.000
0.000
0.000
0.000

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
SAMPLE ID
11G
11H
111
11J
11K
11L
11M
UN
110
IIP
HQ
11R
12A
12B
12C
12D
12E
12F
126
12H
121
12J
12K
12L
12M
12N
120
12P
12Q
12R
13A
13B
13C
13D
13E
13F
13G
13H
131
13J
13K
13L
13M
Cr
0.119
0.180
0.113
n.s.
n.s.
0.050
0.022
0.051
0.028
0.027
0.024
0.040
0.007
n.s.
0.157
0.140
0.150
0.132
0.117
0.164
0.134
0.109
n.s.
0.045
0.042
0.007
0.010
0.031
n.s.
0.050
0.005
n.s.
0.144
0.183
0.123
0.149
0.104
0.135
0.162
0.167
0.166
0.034
0.036
As
0.000
0.000
0.000
n.s.
n.s.
0.017
0.016
0.014
0.015
0.018
0.010
0.021
0.020
n.s.
0.000
0.035
0.000
0.000
0.009
0.000
0.000
0.000
n.s.
0.022
0.019
0.013
0.014
0.015
n.s.
0.015
0.020
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
0.016
Pb
0.000
0.000
0.000
n.s.
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
0.000
0.106
0.000
0.000
0.062
0.000
0.000
0.019
n.s.
0.006
0.000
0.000
0.000
0.000
n.s.
0.000
0.000
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.012
0.001
0.000

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
SAMPLE ID
13N
130
13P
13Q
13R
14A
14B
14C
14D
14E
14F
14G
14H
141
14J
14K
14L
14M
14N
140
14P
14Q
14R
15A
15B
15C
15D
15E
15F
15G
15H
151
15J
15K
15L
15M
15N
150
16A
16B
16C
16D
16E
Cr
0.028
0.003
0.010
0.043
0.032
0.046
n.s.
0.181
0.117
0.188
0.223
0.105
0.203
0.139
0.121
0.160
0.022
0.028
0.008
0.040
0.015
0.038
0.057
0.003
n.s.
n.s.
n.s.
0.153
0.128
0.099
0.135
0.182
0.240
0.175
0.024
0.024
n.S.
n.s.
0.048
n.s.
n.s.
n.s.
0.139
As
0.009
0.014
0.023
0.006
0.016
0.014
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.001
0.000
0.015
0.018
0.020
0.020
0.018
0.014
0.022
0.015
n.s.
n.s.
n.s.
0.000
0.040
0.000
0.000
0.000
0.000
0.000
0.020
0.013
n.s.
n.s.
0.013
n.s.
n.s.
n.s.
0.012
Pb
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
n.s.
n.s.
n.s.
0.000
0.110
0.007
0.000
0.000
0.009
0.000
0.000
0.000
n.s.
n.s.
0.001
n.s.
n.s.
n.s.
0.033

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
SAMPLE ID
Cr
As
Pb
16F
0.177
0.000
0.000
16G
0.177
0.000
0.000
16H
n.s.
n.s.
n.s.
161
0.195
0.000
0.000
16J
0.177
0.000
0.000
16K
0.252
0.000
0.000
16L
n.s.
n. s.
n.s.
16M
n.s.
n.s.
n.s.
16N
n.s.
n.s.
n.s.
160
n.s.
n.s.
n.s.
17A
0.050
0.018
0.000
17B
n.s.
n.s.
n.s.
17C
n.s.
n.s.
n.s.
17D
n.s.
n.s.
n.s.
17E
0.215
0.000
0.000
17F
0.184
0.000
0.000
17G
0.192
0.000
0.000
17H
n.s.
n.s.
n.s.
171
n.s.
n.s.
n.s.
17J
n.s.
n.s.
. s.
17K
n.s.
n.s.
n.s.
17L
n e
n.s.
n.s.
17M
0.024
0.021
0.000
17N
n.s.
n.s.
n.s.
170
n.s.
n.s.
n.s.
18A
0.032
0.026
0.000
18B
n.s.
n.s.
n.s.
18C
n.s.
n.s.
n.s.
18D
n.s.
n.s.
n.s.
18E
0.212
0.000
0.000
18F
0.195
0.000
0.000
18G
0.213
0.000
0.000
18H
M M
n«s«
n.s.
n.s.
181
n.s.
n.s.
n.s.
18J
n.s.
n.s.
n.s.
18K
n.s.
n.s.
n.s.
18L
n.s.
n.s.
n.s.
18M
0.056
0.022
0.000
18N
n.s.
n.s.
n.s.
180
n.s.
n. s.
n.s.
19A
0.060
0.023
0.000
19B
n.s.
n.s.
n.s.
19C
n.s.
n.s.
n.s.

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
SAMPLE ID
Cr
As
Pb
		
		
	
	
19D
n.s.
n.s.
n.s.
19E
0.043
0.024
0.000
19F
0.146
0.005
0.000
19G
0.144
0.000
0.000
19H
n.s.
n.s.
n.s.
191
n.s.
n.s.
n.s.
19J
n.s.
n.s.
n.s.
19K
n.s.
n.s.
n.s.
19L
n.s.
n.s.
n.s.
19M
0.028
0.010
0.000
19N
n.s.
n.s.
n.s.
190
n.s.
n.s.
n.s.
2 OA
0.077
0.016
0.000
20B
n.s.
n.s.
n.s.
20C
n.s.
n.s.
n.s.
20D
n.s.
n.s.
n.s.
20E
0.022
0.013
0.000
20F
0.042
0.017
0.000
20G
0.052
0.013
0.000
2 OH
n.s.
n.s.
n.s.
201
n.s.
n.s.
n.s.
20J
n.s.
n.s.
n.s.
2 OK
n.s.
n.s.
n.s.
20L
n.s.
n.s.
n.s.
20M
n.s.
n.s.
n.s.
2 ON
n.s.
n.s.
n.s.
200
n.s.
n.s.
n.s.
21A
0.049
0.028
0.000
2 IB
n.s.
n.s.
n.s.
21C
n.s.
n.s.
n.s.
2 ID
n.s.
n.s.
n.s.
2 IE
0.055
0.016
0.015
2 IF
0.053
0.011
0.020
21G
0.028
0.015
0.000
21H
n.s.
n.s.
n.s.
211
n.s.
n.s.
n.s.
21J
n.s.
n.s.
n.s.
2 IK
n.s.
n.s.
n.s.
21L
n.s.
n.s.
n.s.
21M
n.s.
n.s.
n.s.
2 IN
n.s.
n.s.
n.s.
210
n.s.
n.s.
n.s.

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
McFarland Non-Grid Points
SAMPLE ID
Cr
As
Pb
Mandated sites


I12-A
0.143
0.000
0.003
L7-A
0.182
0.000
0.000
H3-A
0.230
0.000
0.000
N5-A
0.184
0.000
0.000
Q12-A
0.018
0.016
0.000
M5-A
0.033
0.009
0.000
L5-A
0.066
0.014
0.016
L5-B
0.058
0.018
0.000
L10-A
n.s.
n.s.
n.s.
M5-B
0.041
0.013
0.000
E8-A
0.058
0.017
0.000
H14-A
0.235
0.000
0.000
I9-A
n.s.
n.s.
n.s.
Sites Near
Non-Access
Points

K4-A
0.190
0.000
0.000
K4-B
0.166
0.000
0.000
L4-A
0.209
0.000
0.000
K4-C
0.192
0.000
0.000
M4-A
0.176
0.000
0.000
M4-B
0.191
0.000
0.000
F12-A
0.199
0.000
0.000
L6-A
0.207
0.003
0.009
K4-D
0.056
0.011
0.004

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
XRF Data from Fremont School - Delano. California
SAMPLE ID
Cr
As
Pb
DF1
0.025
0.023
0.000
DF2
0.007
0.024
0.000
DF3
0.048
0.012
0.000
DF4
0.029
0.011
0.000
DF5
0.053
0.010
0.124
DF6
0.028
0.012
0.000
DF7
0.006
0.014
0.000
DF8
0.053
0.013
0.000
DF9
0.076
0.012
0.000
DF10
0.013
0.018
0.000
DF11
0.032
0.024
0.000
DF12
0.018
0.026
0.000
DF13
0.036
0.017
0.000
DF14
0.009
0.022
0.000
DF15
0.028
0.027
0.000
DF16
0.041
0.021
0.000
DF17
0.026
0.016
0.000
DF18
0.012
0.025
0.000
DF19
0.007
0.016
0.000
DF20
0.047
0.014
0.000
DF21
0.026
0.019
0.000
DF22
0.000
0.010
0.000
DF23
0.000
0.018
0.000
DF24
0.010
0.014
0.000
DF25
0.022
0.012
0.000

-------
(Note: n.s. = not sampled due
to inaccessibility or lack: of
permission)
XRF Data from Del Vista School - Delano. California
SAMPLE ID
Cr
As
Pb
DV1
0.030
0.015
0.000
DV2
0.045
0.020
0.000
DV3
0.021
0.018
0.000
DV4
0.054
0.007
0.000
DV5
0.035
0.013
0.000
DV6
0.024
0.013
0.000
DV7
0.016
0.018
0.000
DV8
0.005
0.015
0.000
DV9
0.070
0.009
0.003
DV10
0.034
0.020
0.000
DV11
0.030
0.010
0.000
DV12
0.028
0.015
0.000
DV13
0.031
0.018
0.000
DV14
0.036
0.014
0.000
DV15
0.064
0.019
0.000
DV16
0.041
0.016
0.000
DV17
0.051
0.017
0.000
DV18
0.062
0.020
0.000
DV19
0.024
0.024
0.000
DV20
0.013
0.020
0.000

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
XRF Data from Montibello Rose Co. - McFarland. California
SAMPLE ID
Cr
As
Pb
MR1
0.035
0.011
0.000
MR2
0.035
0.063
0.000
MR3
0.054
0.058
0.001
MR4
0.019
0.052
0.000
MR5
0.018
0.039
0.000
MR6
0.016
0.036
0.003
MR7
0.015
0.059
0.000
MR8
0.035
0.020
0.000
MR9
0.058
0.015
0.001
MR10
0.033
0.024
0.000
MRU
0.023
0.021
0.000
MR12
0.019
0.025
0.000
MR13
0.080
0.021
0.020
MR14
0.048
0.015
0.000
MR15
0.046
0.023
0.008

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
XRF Data from Potato Plant Area - McFarland. California
SAMPLE ID
Cr
As
Pb
PP1
0.043
0.018
0.000
PP2
0.017
0.012
0.000
PP3
0.032
0.016
0.000
PP4
0.040
0.024
0.000
PP5
0.037
0.014
0.000
PP6
0.018
0.018
0.000
PP7
0.019
0.014
0.000
PP8
0.001
0.023
0.000
PP9
0.020
0.023
0.000
PP10
0.046
0.012
0.019
PP11
0.029
0.025
0.000
PP12
0.026
0.021
0.000
PP13
0.032
0.018
0.000

-------
(Note: as. = not sampled due
to inaccessibility or lack of
permission)
XRF Data from Well No. 5 - McFarland. California
SAMPLE ID
Cr
As
Pb
5W1
0.000
0.020
0.000
5W2
0.002
0.020
0.000
5W3
0.017
0.015
0.002
5W4
0.007
0.022
0.000
5W5
0.022
0.007
0.008
5W6
0.015
0.010
0.001
5W7
0.046
0.018
0.000
5W8
0.022
0.019
0.000
5W9
0.008
0.022
0.000
5W10
0.017
0.021
0.000
5W11
0.010
0.018
0.000
5W12
0.022
0.026
0.000

-------
(Note: n.s. = not sampled due
to inaccessibility or lack of
permission)
XRF Data from Well No.	6 - McFarland. California
SAMPLE ID	Cr	As	Pb
1	0.150	0.000	0.000
2	0.248	0.000	0.000
3	0.191	0.000	0.000
4	0.228	0.000	0.000
5	0.190	0.000	0.000
6	0.137	0.000	0.000
7	0.221	0.000	0.000
8	0.193	0.000	0.000
9	0.174	0.000	0.000
10	0.237	0.000	0.000
11	0.127	0.000	0.000
12	0.144	0.000	0.000
13	0.163	0.000	0.000
14	0.133	0.000	0.000
15	0.116	0.000	0.000
16	0.132	0.000	0.000
17	0.141	0.000	0.000
18	0.167	0.000	0.000
19	0.196	0.000	0.000
20	0.144	0.000	0.000
21	0.056	0.000	0.007
22	0.220	0.000	0.000

-------
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SAMPLING TEAM - A
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JULY 1989

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-------
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:
-------
Appendix 2
SOIL SAMPLING
McFarland, California
B1

-------
Soil Sampling in McFarland, California
Samples were taken by Kevin Cabbie and Chris Carlsen
Soil sampling at McFarland, California began July 20, 1989
and was completed July 22, 1989. The sample identification
number, location, soil temperature, and the size of the area
sampled was recorded for each of the sample locations. The soil
sampling location identification numbers were taken from the XRF
sampling grid (Figure 1) developed by the California Department
of Health Services (CDHS). This map grid consists of letters
along the northern border and numbers along the eastern border.
The soil "Sample ID" consist of these coordinates with a two
digit numeral identification appended to the end.
Example: SAMPLE ID# D802
"D" - indicates the sample was located along the
north - south sampling line designated "D".
"8" - indicates it was located along the east - west
line number "8".
"02" - indicates the soil sample was the second sample
collected.
Once all soil sampling sites were located by CDHS and
Region 9 personnel, it was determined whether each site had
fertilizers or pesticides applied to it. If either of these
products were used, the site was not sampled.
The sampling equipment consisted of a stainless steel spoon,
trowel, and a #10 mesh screen. The equipment was decontaminated
after each use by brushing with Alconox® in a stainless steel
pan. Equipment was then rinsed, first with deionized water, next
with an acid rinse (0.1M HC1), then with reagent water, and
finally with a methanol rinse. Decontaminated equipment was
wrapped in aluminum foil to prevent accidental contamination
between uses.
The sampling procedure consisted of selecting a relatively
vegetation-free 6 inch by 6 inch area and clearing away all
surface debris. The samples were collected using a stainless
steel spoon and trowel. The two semi-volatile (SVO) samples were
spooned directly into two 125ml clear glass containers. The
pesticide and inorganic samples were collected by sieving the
soil with the #10 sieve to remove all organic material in the
sample. This soil was collected in an aluminum pan and mixed
together to form a composite sample. The composite sample was
spooned into two bottles, a 125ml clear glass bottle for
pesticide analysis and a 250ml amber polypropylene bottle for
inorganic analysis. All sample bottles were sealed and placed in

-------
a cooler with the temperature maintained at 4°C using Kool-lt®
ice packs. Samples were stored in a portable refrigerator with a
maintained temperature of 4"C overnight, prior to shipment to the
laboratory.
The sampling team maintained a field logbook detailing
sampling activities. The following is a summary of these
activities.
SAMPLE ID* DF01
Taken by Ken Scarbrough
Kevin Cabbie
Chris Carlsen
Date 07/20/89
Began sampling at 15:46
Completed sampling at 16:45
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125 ml
1 inorganic -> 250ml
Soil temperature: 38°C
The first sample, ID# DF01, was taken for use as a
background sample for McFarland. This sample was taken
approximately 10 miles north of McFarland at Fremont School in
Delano, California.
SAMPLE ID# D802
Taken by Ken Scarbrough
Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began sampling at 8:48
Completed sampling at 09:00
Sample ID# D802 was taken
located in grid section D8. T
of the property, in an area of
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 29"C
from the front yard of a house
e sample was taken near the center
exposed soil by the front door.
SAMPLE ID# P803
Taken by Ken Scarbrough
Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began Sampling at 09:37
Completed sampling at 10:05
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 32°C
Sample ID# P803 was taken from the front of a house locatejd
in grid section P8. The sample was taken from an area of exposed
soil on the right side of the car port.

-------
Sample ID IF1204
Taken by Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began sampling at 12:45
Completed sampling at 13:12
Sample ID# F1204 was tak
backyard of a house located i
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 36*C
n from the far left corner of the
; grid section F12.
SAMPLE ID# 11205
Taken by Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began sampling at 13:26
Completed sampling at 13:57
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 38*C
Sample ID# 11205 was taken from the middle of the backyard
of a house located in grid section 112. The sample was taken
from a grass covered area near a cactus growing in exposed soil.
SAMPLE ID# M4A06
Taken by Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began sampling at 14:10
Completed sampling at 14;
45
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 38*C
Sample ID# M4A06 was taken near the fence, in the middle of
the backyard of a house located in grid section M4.
SAMPLE ID# L4A07
Taken by Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began sampling 14:50
Completed sampling at 15:10
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 40°C
Sample ID# L4A07 was taken from a house located in grid
section L4. The sample was taken from the right side of the
front yard near the fence.

-------
SAMPLE ID# M14A08
Taken by Ken Scarbrough
Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began sampling at 16:37
Completed sampling at 17:03
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 42°C
Sample ID# M14A08 was collected in grid section M14. A high
XRF reading was reported at this location. The sample was taken
in the drainage ditch approximately 25 feet east of the railroad
tracks.
SAMPLE ID# H709
Taken by Ken Scarbrough
Kevin Cabbie
Chris Carlsen
Date 07/21/89
Began sampling at 17:35
Completed sampling at 18:25
Sample ID# H709 was take
backyard of a house located i
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 4l°c
from the left corner of the
grid section H7.
SAMPLE ID# M510
Taken by Kevin Cabbie
Chris Carlsen
Date 07/22/89
Began sampling at 08:35
Completed sampling at 09:14
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 3 3°C
Sample ID# M510 was taken from the center of the north end
of the backyard of a house located in grid section M5.
SAMPLE ID# K411
Taken by Kevin Cabbie
Chris Carlsen
Date 07/22/89
Began sampling at 9:15
Completed sampling at 09:55
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 34°C
Sample ID# K411 was taken from the right corner of the
backyard of a house located in grid section K4.

-------
SAMPLE ID# J212
Taken by Kevin Cabbie
Chris Carlsen
Date 7/22/89
Began sampling at 11:40
Completed sampling at 12:30
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 38*C
Sample ID# J212 was taken at the bottom of the potato
washing pit located in grid section J2. Three samples were taken
at the bottom of the pit to make up a composite sample. These
samples were taken at the north end and the middle of the pit.
An organic layer of decomposed plants and material was laying on
the surface of the pit. This layer was removed to reach the soil
for sampling.
SAMPLE ID# L513
Taken by Kevin Cabbie
Chris Carlsen
Date 07/22/89
Began sampling at 13:00
Completed sampling at 14:15
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 44*
Sample ID# L513 was taken at the McFarland city sump, grid
section L5. The SVO grab sample was taken at the discharge area
at Glenwood Street at the east side of the sump. The pesticide
and inorganic samples were a composite sample taken from the
south end of the sump, the discharge area at Glenwood Street, and
the purge water discharge area from well #5 located in the sump
area on the north side.
SAMPLE ID# D414
Taken by Kevin Cabbie
Chris Carlsen
Date 07/22/89
Began sampling at 14:25
Completed sampling at 14:55
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 45°C
Sample ID# D414 was taken at the McFarland city water well
#6, grid section D4. The sample was taken on the northwest
corner of the fenced area around well #6. The sample area was on
the west side of the fence.
SAMPLE ID# P715
Taken by Kevin Cabbie
Chris Carlsen
Date 07/22/89
Began sampling at 15:10
Completed sampling at 15:3
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 38*C

-------
Sample ID# P715 was taken at Browning School in McFarland,
grid section P7. The sample was taken from the northeast section
of the fenced playground area, oh the east side of the fence.
SAMPLE ID# N116
Taken by Kevin Cabbie
Chris Carlsen
Date 07/22/89
Began sampling 16:45
Completed sampling at 17:15
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 47 *C
Sample ID# N116 was taken at Elmo Road between State Route
99 and Browning Road in McFarland, grid section Nl. The three
point composite sample was taken between Browning Road and state
Route 99 along Elmo road approximately 10 feet off the road, next
to the cotton field. Samples were taken near the middle, and at
both ends of the field.
SAMPLE ID# R1417
Taken by Kevin Cabbie
Chris Carlsen
Date 07/22/89
Began sampling at 17:25
Completed sampling at 18:0
Samples taken:
2 SVO -> 125/250ml (total sample)
1 Pesticide -> 125ml
1 Inorganic -> 250ml
Soil temperature: 46*C
Sample ID# R1417 was taken at the intersection of Wiley and
Sherwood Road in McFarland, grid section R14. The sample was
collected from the east side of Wiley Road, approximately 30
meters from Sherwood Road.

-------
e

0MtRM»O «>•
1000
feci
JULY 1909
977000
97BOOO
979000
980000
967000
903000
981000
MCFflRLflND XRF SAMPLING GRID
Figure 1

-------
Appendix 3
INORGANIC CHEMICAL ANALYSES
McFarland, California
CI

-------
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: LQCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	 SDG No.: D414.
SOW No.: 787	
EPA Sample No.	Lab Sample ID.
	D414		E89S017
	D802		E89S020
	DF01		E89S014
	F1204		E89S021	
	H709		E89S018	
	11205		E89S016
	J212		E89S025
	K411		E89S013
	L4A07		E89S012
	L513		E89S022	
	M14A08		E89S023
	M4A06		E89S015
	MS 10		E89S011	
	M51Q	D_	E89S029D	
	M51Q	S	E89S028S	
	N116	I	E89S027
	P715		E89S019	
	P803		E89S024
R1417	E89S026
Were ICP iriterelement corrections applied ?
Were ICP background corrections applied ?
If yes - were raw data generated before
application of background corrections ?
Yes/No N0_
Yes/No YES
Yes/NO N0_
Comments:
Release of the data contained in this hardcopy data package and in the
computer-readable data submitted on floppy diskette has been authorized by
the Laboratory Manager or the Manager's designee, as verified by the
following signature.
Lab Manager:		'/£,/( 		
Date: 	
COVER PAGE - IN	7/87

-------
U.S. EPA - CLP
1	EPA SAMPLE M.
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED ESC		Contract: 68-03-3 249
D414
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	 SDG No.: D414_
Matrix (soil/water) : SOIL_	Lab Sample ID: E89S01^_
Level (low/med):			Date Received: 07/25/89
% Solids:	_99.9
Concentration Units (ug/L or mg/kg dry weight): MG/KG
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
6440


P
7440-36-0
Antimony_
Arsenic
12.0
U
N
P
7440-38-2
2.0


F
7440-39-3
Barium
67 . 3


P
7440-41-7
Beryllium
0.87
B

P
7440-43-9
Cadmium
2.2


P
7440-70-2
Calcium
3760


P
7440-47-3
Chromium
17.3


P
7440-48-4
Cobalt
12.2


P
7440-50-8
Copper
15.5


P
7439-89-6
Iron
9350


P
7439-92-1
Lead .
6.2

S
F
7439-95-4
Magnesium
2780


P
7439-96-5
Manganese
178


P
7439-97-6
Mercury	
Nickel
0. 16


AV
7440-02-0
8.9


P
7440-09-7
Potassium
2730


A
7782-49-2
Selenium
0.40
U

F
7440-22-4
Silver
2.2


P
7440-23-5
Sodium
368
B

P
7440-28-0
Thallium
0 .40
U

F
7440-62-2
Vanadium
26.4


P
7440-66-6
Zinc
48.2


P
	—	
Cyanide



NR






Color Before: 	.	Clarity Before: 		Texture: MEBI
Color After: 		Clarity After: 		Artifacts: 	
Comments:
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): SOIL_
Level (low/med):		
\ Solids:	95.1
EPA SAMPLE NO.
D802
SDG No.: D414
Lab Sample ID: E89S020_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
2olor Before:
Color After:
Comments:
CAS No.
Analyte
Concentration
C
Q
7429-90-5
Aluminum
8420


7440-36-0
Antimony_
Arsenic
12.6
U
N
7440-38-2
2.4


7440-39-3
Barium
115


7440-41-7
Beryllium
Cadmium
0.32
u

7440-43-9
0.84
u

7440-70-2
Calcium
7250


7440-47-3
Chromium
14.7


7440-48-4
Cobalt
7.1
B

7440-50-8
Copper
12.7


7439-89-6
Iron
11600


7439-92-1
Lead
8.0


7439-95-4
Magnesium
3980


7439-96-5
Manganese
249


7439-97-6
Mercury
Nickel
0.14
U

7440-02-0
9.9


7440-09-7
Potassium
3260


7782-49-2
Selenium
0.42
U

7440-22-4
Silver
1.1
B

7440-23-5
Sodium
663
B

7440-28-0
Thallium
0.42
U

7440-62-2
Vanadium
31.2


7440-66-6
Zinc
43.0


	
Cyanide








Clarity Before:
Clarity After:
M
¥Z
P_
F_
P_
P_
P_
P_
P_
P_
P_
P_
F_
P_
P_
AV
P_
A_
F_
P_
P_
F_
P_
P_
NR
Texture:
Artifacts:
MEDIUM
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): SOIL_
Level (low/med):		
% Solids:	98.1
EPA SAMPLE N
I
DF01
SDG No.: D414
Lab Sample ID: E89SOI4J.
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
Clarity Before:
Clarity After:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
7230


P
7440-36-0
Antimony_
Arsenic
12.2
U
N
P
7440-38-2
2.3


F
7440-39-3
Barium
113


P
7440-41-7
Beryllium
Cadmium
0.31
U

P
7440-43-9
0.82
U

P
7440-70-2
Calcium
2960


P
7440-47-3
Chromium
11.6


P
7440-48-4
Cobalt
6.0
B

P
7440-50-8
Copper
10.2


P
7439-89-6
Iron
10500


P
7439-92-1
Lead
9.9


F
7439-95-4
Magnesium
3100


P
7439-96-5
Manganese
238


P
7439-97-6
Mercury
Nickel
0.15


AV
7440-02-0
20.6


P
7440-09-7
Potassium
3490


A
7782-49-2
Selenium
0.41
U

F
7440-22-4
Silver
1.6
B

P
7440-23-5
Sodium
581
B

P
7440-28-0
Thallium
0.41
U

F
7440-62-2
Vanadium
27.9


P
7440-66-6
Zinc
34.2


P
	
Cyanide



NR






Texture: ME
Artifacts:
V
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.:
EPA SAMPLE NO.
F1204
SDG No.: D414
Matrix (soil/water): S0IL_
Level (low/med): 	
% Solids:	98.0
Lab Sample ID: E89S021_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentration
C
Q
7429-90-5
Aluminum
6600


7440-36-0
Antimony_
Arsenic
12.2
U
N
7440-38-2
14.1


7440-39-3
Barium -
102


7440-41-7
Beryllium
Cadmium
0.31
u

7440-43-9
0.82
u

7440-70-2
Calcium
3570


7440-47-3
Chromium
28.3


7440-48-4
Cobalt
6.5
B

7440-50-8
Copper
15.0


7439-89-6
Iron
9860


7439-92-1
Lead
86.7

S
7439-95-4
Magnesium
3010


7439-96-5
Manganese
223


7439-97-6
Mercurv
0.15


7440-02-0
Nickel
10.9


7440-09-7
Potassium
3620


7782-49-2
Selenium
0.41
U

7440-22-4
Silver
1.0
U

7440-23-5
Sodium
380
B

7440-28-0
Thallium
0.41
U

7440-62-2
vanadium
26.5


7440-66-6
Zinc
97.8


		
Cyanide





¦


M
P^
P_
F_
P_
P_
P_
P_
P_
P_
P_
P_
F_
P_
P_
AV
P_
A_
F_
P_
P_
F_
P_
P_
NR
Clarity Before:
Clarity After:
Texture:
Artifacts:
MEDIUM
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.:
EPA SAMPLE N
I
H709
Matrix (soil/water): SOIL_
Level (low/med):		
% Solids:	99.9
	 SDG No.: D414_
Lab Sample ID: E89S018^_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
Clarity Before:
Clarity After:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
8600


P
7440-36-0
Antimony_
Arsenic
12.0
U
N
P
7440-38-2
3.3


F
7440-39-3
Barium
85.8


P""
7440-41-7
Beryllium
0.65
B

P
7440-43-9
Cadmium
1.7


P
7440-70-2
Calcium
3460


P
7440-47-3
Chromium
16.6


P
7440-48-4
Cobalt
8.7
B

P
7440-50-8
Copper
14.4


P
7439-89-6
Iron
11900


P
7439-92-1
Lead
31.1


F
7439-95-4
Magnesium
3610


P
7439-96-5
Manganese
228


P
7439-97-6
Mercury
0.14
U

AV
7440-02-0
Nickel
15.5


P
7440-09-7
Potassium
4150


A
7782-49-2
Selenium
0.40
u

F
7440-22-4
Silver
2 . 2


P
7440-23-5
Sodium
483
B

P
7440-28-0
Thallium
0.40
U

F
7440-62-2
Vanadium
32.5

P
7440-66-6
Zinc
58.2


P
—	
Cyanide



NR






Texture: MELT
Artifacts:
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.:
EPA SAMPLE NO.
SDG No.: 0414
Matrix (soil/water): SOIL_
Level (low/med):		
% Solids:
Lab Sample ID: E89S016_
Date Received: 07/25/89
100.0
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentrat ion
C
Q
M
7429-90-5
Aluminum
10400


P
7440-36-0
Antimony_
Arsenic
12.0
U
N
P
7440-38-2
3.8


F
7440-39-3
Barium
123


P
7440-41-7
Beryllium
Cadmium
0.32
B

P
7440-43-9
0.80
U

P
7440-70-2
Calcium
4570


P
7440-47-3
Chromium
16.5


P
7440-48-4
Cobalt
6.9
B

P
7440-50-8
Copper
17.0


P
7439-89-6
Iron
14200


P
7439-92-1
Lead
96.3


F
7439-95-4
Magnesium
4150


P
7439-96-5
Manganese
284


P
7439-97-6
Mercury
Nickel
0.23


AV
7440-02-0
19.9


P
7440-09-7
Potassium
4980


A
7782-49-2
Selenium
0.40
U

F
7440-22-4
Silver
1.0
U

P
7440-23-5
Sodium
400
B

P
7440-28-0
Thalli\;m_
Vanadium
0.40
U

F
7440-62-2
28.8


P
7440-66-6
Zinc
131


P
			
Cyanide



NR






Clarity Before:
Clarity After:
Texture: MEDIUM
Artifacts: 	
FORM I - IN
7/87

-------
U.S. EPA - CLP
INORGANIC ANALYSES DATA SHEET
EPA SAMPLE
Contract: 68-03-3249
Lab Name: LOCKHEED_ESC	
Lab Code: LESC		Case No.:MCFARLAND SAS No.:
Matrix (soil/water): SOIL_
Level (low/med): 	
% Solids:	99.8
1
K411
SDG No.: D414
Lab Sample ID: E89S012^
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
10300


P
7440-36-0
Antimony_
Arsenic
14.5

N
P
7440-38-2
2.6


F
7440-39-3
Barium
104


P
7440-41-7
Beryllium
0.30
U

P
7440-43-9
Cadmium
0.80
u

P
7440-70-2
Calcium
3220


P
7440-47-3
Chromium
13.8


P
7440-48-4
Cobalt
7.1
B

P
7440-50-8
Copper
10.9


P
7439-89-6
Iron
13600


P
7439-92-1
Lead
12.2


F
7439-95-4
Magnesium
4130


P
7439-96-5
Manganese
270


P
7439-97-6
Mercury
0. 14
U

AV
7440-02-0
Nickel
12.1


P
7440-09-7
Potassium
3710


A
7782-49-2
Selenium
0.40
u

F
7440-22-4
Silver
1.1
B

P
7440-23-5
Sodium
516
B

P
7440-28-0
Thallium
0.40
U

F
7440-62-2
Vanadium
29.8


P
7440-66-6
Zinc
36.9


P
		
Cyanide



NR






Clarity Before:
Clarity After:
Texture: MEC,T.i
Artifacts:
FORM I - IN
7/87

-------
U.S. EPA •- CLP
1
INORGANIC ANALYSES DATA SHEET
|ib Name: LOCKHEED_ESC	 Contract: 68-03-3249
,ab Code: LESC	Case No.:MCFARLAND SAS No.: 	
EPA SAMPLE NO.
I
r:
SDG No.: D414
litrix (soil/water) : SOIL_
avel (low/med):		
Solids:	100.0
Lab Sample ID: E89S025_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
¦slor Before:
tolor After:
"imments:
Clarity Before:
Clarity After:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
18500
U

P
7440-36-0
Antimony_
Arsenic
12.0
N
P
7440-38-2
7.1


F
7440-39-3
Barium
190


P
7440-41-7
Beryllium
Cadmium
0.54
B

P
7440-43-9
0.80
U

P
7440-70-2
Calcium
4360


P
7440-47-3
Chromium
27.8


P
7440-48-4
Cobalt
12.5


P
7440-50-8
Copper
26.7


P
7439-89-6
Iron
26600


P
7439-92-1
Lead
14.5


F
7439-95-4
Magnesium
8160


P~
7439-96-5
Manganese
313


P	
7439-97-6
Mercury
Nickel
1.8


AV
7440-02-0
18.9


P
7440-09-7
Potassium
7490


A
7782-49-2
Selenium
0.40
U

F
7440-22-4
Silver
1.0
U

P
7440-23-5
Sodium
518
B

P
7440-28-0
Thallium
0.40
U

F
7440-62-2
Vanadium
64.5


P
7440-66-6
Zinc
128


P

Cyanide	



NR





Texture: MEDIUM
Artifacts: 		
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHSED_ESC	 Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.:
EPA SAMPLE NO.
L4A07
SDG No.: D414
Matrix (soil/water): SOIL_
Level (low/med): 	
% Solids:	100.0
Lab Sample ID: E89SQ12_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS NO.
Analyte
Concentration
C
Q
7429-90-5
Aluminum
8410
u

7440-36-0
Antimony
12.0
N
7440-38-2
Arsenic
2.6


7440-39-3
Barium
99.8


7440-41-7
Beryllium
Cadmium
0.30
U

7440-43-9
0.80
u

7440-70-2
Calcium
2470


7440-47-3
Chromium
12.5


7440-48-4
Cobalt
7.1
B

7440-50-8
Copper
10.3


7439-89-6
Iron
11900


7439-92-1
Lead
5.3


7439-95-4
Magnesium
3830


7439-96-5
Manganese
240


7439-97-6
Mercury
Nickel
0.14
U

7440-02-0
12.5


7440-09-7
Potassium
3350
u

7782-49-2
Selenium
0.40

7440-22-4
Silver
1.5
B

7440-23-5
Sodium
398
B

7440-28-0
Thallium
0.40
U

7440-62-2
Vanadium
28.5


7440-66-6
Zinc
35.5


_____		
Cyanide	







Clarity Before;
Clarity After:
M
__
P_
F_
P_
P_
P_
P_
P_
P
P~
P~
F_
?_
P_
AV
P
AI
F_
P_
P_
F_
P_
P_
NR
Texture: MEDIUM
Artifacts: 	
v
FORM I - IN
7/87

-------
.U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): SOIL_
Level (low/med):		
% Solids:	97.6
EPA SAMPLE N'
L513
SDG No.: D4]
Lab Sample ID: E89S02
Date Received: 07/25/
1
l
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
9820


P
7440-36-0
Antimony_
Arsenic
12.3
U
N
P
7440-38-2
8.3


F
7440-39-3
Barium
115


P
7440-41-7
Beryllium
Cadmium
0.36
B

p"
7440-43-9
0.82
U

P
7440-70-2
Calcium
4160


P
7440-47-3
Chromium
15.3


P
7440-48-4
Cobalt
6.8
B

P
7440-50-8
Copper
12.3


P
7439-89-6
Iron
14000


P
7439-92-1
Lead
8.5

S
F
7439-95-4
Magnesium
4540


P
7439-96-5
Manganese
244


P
7439-97-6
Mercury
Nickel
0. 13
U

AV
7440-02-0
9.4


P
7440-09-7
Potassium
3480


A
7782-49-2
Selenium
0.41
U

F
7440-22-4
Silver
1.0
U

P
7440-23-5
Sodium
400
B

P
7440-28-0
Thallium
0.41
U

F
7440-62-2
Vanadium
33.6


P
7440-66-6
Zinc
49.4


P
		—-—
Cyanide



NR

—




Clarity Before:
Clarity After:
Texture: MEDI
Artifacts:
FORM. I - IN
7/37

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): SOIL_
Level (low/med): 	
% Solids:	99.6
EPA SAMPLE NO.
M14A08
SDG No.: 0414
Lab Sample ID: E89S023_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentrat ion
C
Q
7429-90-5
Aluminum
14600


7440-36-0
Antimony_
Arsenic
12.0
U
N
7440-38-2
254


7440-39-3
Barium
198


7440-41-7
Beryllium
Cadmium
0.50
B

7440-43-9
0.80
U

7440-70-2
Calcium
7510


7440-47-3
Chromium
27.7


7440-48-4
Cobalt
12.4


7440-50-8
Copper
332


7439-89-6
Iron
27600


7439-92-1
Lead
222


7439-95-4
Magnesium
6640


7439-96-5
Manganese
491


7439-97-6
Mercury
1.3


7440-02-0
Nickel
32.3


7440-09-7
Potassium
5830


7782-49-2
Selenium
0.40
U

7440-22-4
Silver
1.1
B

7440-23-5
Sodium
577
B

7440-28-0
Thallium
1.3
B

7440-62-2
Vanadium
48.5


7440-66-6
Zinc
477


		—
Cyanide








Clarity Before:
Clarity After:
M
P_
P_
F_
P_
P_
P_
P_
P_
P_
P_
P_
P_
P_
P_
AV
P_
A_
F_
P_
P_
F
P~
P_
NR
Texture:
Artifacts:
MEDIUM
FORM I - IN
7/87

-------
•U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.:
EPA SAMPLE
M4A06
SDG No.: D414
Matrix (soil/water): S0IL_
Level (low/med):		
% Solids:	96.6
Lab Sample ID: E89S01^|
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
9830


P
7440-36-0
Antimony_
Arsenic
12.4
U
N
P
7440-38-2
2.8


F
7440-39-3
Barium
110


P
7440-41-7
Beryllium
Cadmium
0.35
B

P
7440-43-9
0.83
U

P
7440-70-2
Calcium
3760


P
7440-47-3
Chromium
15.2


P
7440-48-4
Cobalt
8.1
B

P
7440-50-8
Copper
12.9


P
7439-89-6
Iron
13500


P
7439-92-1
Lead
7.5


F
7439-95-4
Magnesium
4250


P
7439-96-5
Manganese
292


P
7439-97-6
Mercury	
Nickel
0.26


AV
7440-02-0
11.9


P
7440-09-7
Potassium
3820


A
7782-49-2
Selenium
0.41
U

F
7440-22-4
Silver
1.4
B

P
7440-23-5
Sodium
541
B

P
7440-28-0
Thallium
0.48
B

F
7440-62-2
Vanadium
33.7


P
7440-66-6
Zinc
38.0


P
	
Cyanide



NR






Clarity Before:
Clarity After:
Texture: MEDi
Artifacts:
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water) : SOIL_
Level (low/med):		
% Solids:	95.1
EPA SAMPLE NO.
M510
SDG No.: D414
Lab Sample ID: E89S0ll_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentration
C
Q
7429-90-5
Aluminum
8490


7440-36-0
Antimony_
Arsenic
12.6
U
N
7440-38-2
1.9
B

7440-39-3
Barium
96.6
U

7440-41-7
Beryllium
Cadmium
0.32

7440-43-9
0.84
u

7440-70-2
Calcium
3320


7440-47-3
Chromium
12.9


7440-48-4
Cobalt
6.1
B

7440-50-8
Copper
12.2


7439-89-6
Iron
13100


7439-92-1
Lead
15.6


7439-95-4
Magnesium
3670


7439-96-5
Manganese
243


7439-97-6
Mercury
Nickel
0.14
U

7440-02-0
9.5


7440-09-7
Potassium
3820


7782-49-2
Selenium
0.42
u

7440-22-4
Silver
1.1
u

7440-23-5
Sodium
380
B

7440-28-0
Thallium
0.46
B

7440-62-2
Vanadium
26.7


7440-66-6
Zinc
63.0



Cyanide












Clarity Before:
Clarity After:
M
P_
P_
F_
P_
P_
P_
P_
P_
P_
P_
P_
F_
P_
P_
AV
P_
A_
F_
P_
P_
F_
P_
P_
NR
Texture: MEDIUM
Artifacts: 	
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): SOIL_
Level (low/med):		
% Solids:	99.8
EPA SAMPLE n|.
N116
SDG No.: D414
Lab Sample ID: E89S027
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
5070


P
7440-36-0
Antimony_
Arsenic
12.0
U
N
P
7440-38-2
2.1


F
7440-39-3
Barium
55.0


P
7440-41-7
Beryllium
Cadmium
0.30
U

P
7440-43-9
0.80
U

P
7440-70-2
Calcium
1640


P
7440-47-3
Chromium
11.3


P
7440-48-4
Cobalt
4.0
B

P
7440-50-8
Copper
6.7


P
7439-89-6
Iron
7190


P
7439-92-1
Lead
26.5

S
F
7439-95-4
Magnesium
2050


P
7439-96-5
Manganese
156


P
7439-97-6
Mercury
Nickel
0.13
U

AV
7440-02-0
7.5
B

P
7440-09-7
Potassium
2160
U

A
7782-49-2
Selenium
0.40

F
7440-22-4
Silver
1.0
u

P
7440-23-5
Sodium
251
B

P
7440-28-0
Thallium
0.40
U

F
7440-62-2
Vanadium
17.1


P
7440-66-6
Zinc
30.1


P
	
Cyanide



NR






Clarity Before:
Clarity After:
Texture: ME£J
Artifacts:
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.:
EPA SAMPLE NO.
P715
SDG No.: D414
Matrix (soil/water): SOIL_
Level (low/med):		
% Solids:	99.3
Lab Sample ID: E89S019_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
Clarity Before:
Clarity After:
CAS No.
Analyte
Concentration
C
Q
M
7429-90-5
Aluminum
11500
U

P
7440-36-0
Antimony
12.1
N
P
7440-38-2
Arsenic
2.5


F
7440-39-3
Barium -
98.4


P
7440-41-7
Beryllium
Cadmium
0.80
B

P
7440-43-9
1.4


P
7440-70-2
Calcium
3070


P
7440-47-3
Chromium
24.7


P
7440-48-4
Cobalt
13.3


P
7440-50-8
Copper
20.6


P
7439-89-6
Iron
15400


P
7439-92-1
Lead
8.7


F
7439-95-4
Magnesium
4370


P
7439-96-5
Manganese
355


P
7439-97-6
Mercury
0.25


AV
7440-02-0
Nickel
20.3


P
7440-09-7
Potassium
4010


A
7782-49-2
Selenium
0.40
U

F
7440-22-4
Silver
1.6
B

P
7440-23-5
Sodium
442
B

P
7440-28-0
Thallium
0.40
U

F
7440-62-2
Vanadium
39.5


P
7440-66-6
Zinc
48.9


P
	
Cyanide



NR






Texture: MEDIUM
Artifacts:
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.:
Matrix (soil/water): SOIL_
Level (low/med):		
% Solids:	98.3
EPA SAMPLE
1
P803
SDG No.: D414
Lab Sample ID: E89S02|_
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS NO.
Analyte
Concentration
C
Q
7429-90-5
Aluminum
6850


7440-36-0
Antimony_
Arsenic
12.2
U
N
7440-38-2
1.9
B
S
7440-39-3
Barium
148


7440-41-7
Beryllium
Cadmium
0.31
U

7440-43-9
0.81
u

7440-70-2
Calcium
4260


7440-47-3
Chromium
13 .7


7440-48-4
Cobalt
5.8
B

7440-50-8
Copper
17.8


7439-89-6
Iron
10100


7439-92-1
Lead
72.2


7439-95-4
Magnesium
2830


7439-96-5
Manganese
226


7439-97-6
Mercury	
Nickel
0.37


7440-02-0
15.0


7440-09-7
Potassium
2710


7782-49-2
Selenium
0.41
U

7440-22-4
Silver
1.0
U

7440-23-5
Sodium
650
B

7440-28-0
Thallium
0.41
U

7440-62-2
Vanadium
23.4


7440-66-6
Zinc
131


——	
Cyanide








Clarity Before:
Clarity After:
M
P_
P_
F_
P_
P_
P_
P_
P_
P_
P_
P_
F_
P_
P_
AV
P_
A_
F__
P_
P_
F_
P_
P_
NR
Texture: MET1
Artifacts:
FORM I - IN
7/87

-------
U.S. EPA - CLP
1
INORGANIC ANALYSES DATA SHEET
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): SOIL_
Level (low/med): 	
i Solids:	99.8
EPA SAMPLE NO.
R1417
SDG No.: D414
Lab Sample 10: E89S026__
Date Received: 07/25/89
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Color Before:
Color After:
Comments:
CAS NO.
Analyte
Concentration
C
Q
7429-90-5
Aluminum
8220


7440-36-0
Antimony_
Arsenic
13.9

N
7440-38-2
2.4


7440-39-3
Barium
86.4


7440-41-7
Beryllium
Cadmium
0.32
B

7440-43-9
0.80
U

7440-70-2
Calcium
2630


7440-47-3
Chromium
15.3


7440-48-4
Cobalt
7.2
B

7440-50-8
Copper
13.1


7439-89-6
Iron
11700


7439-92-1
Lead
16.6


7439-95-4
Magnesium
3380


7439-96-5
Manganese
305


7439-97-6
Mercury
0.15
U

7440-02-0
Nickel
13.8


7440-09-7
Potassium
3140


7782-49-2
Selenium'
0.40
U

7440-22-4
Silver
1.0
U

7440-23-5
Sodium
394
B

7440-28-0
Thallium
0.40
U

7440-62-2
Vanadium
29.4


7440-66-6
Zinc
40.8


	—-
Cyanide








Clarity Before:
Clarity After:
M
P_
P_
F_
P_
P_
P_
P_
P_
P_
P_
P
F~
P_
P_
AV
P_
A_
F_
P_
P_
F_
P_
P_
NR
Texture:
Artifacts:
MEDIUM
FORM I - IN
7/87

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No. : MCFARLAND SAS No.: 	 SDG No.:
Initial Calibration Source: EMSL-LV,NBS
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial Calibration

Continuing Calibration
1
J
True
Found
%Rd)
True
Found
%R(1)
Found
%R(iW
Aluminum
2000.0
2057.74
102.9
10000.0
10158.23
101.6
10318.92
103 . M
Antimony_
1010.0
995.00
98.5
5000.0
5154.64
103.1
5045.38
100. ¦
Arsenic
100.0
97.40
97.4
50.0
51.10
102.2
47.40
94 . K
Barium
2010.0
1882.59
93.7
2500.0
2428.25
97. 1
2496.75
99.9]
Beryllium
501.0
482.31
96.3
500.0
492.18
98 . 4
502.15
100. ¦
Cadmium
492.0
473.04
96.1
2500.0
2448.18
97.9
2444.88
97.1
Calcium
50200.0
50248.63
100.1
25000.0
25234.29
100.9
25532.36
102. n
Chromium
503.0
483.37
96.1
5000.0
4753.25
95.1
4915.04
98.31
Cobalt
498.0
486.58
97.7
5000.0
4882.42
97.6
4991.59
99. ¦
Copper
520.0
490.43
94.3
5000.0
4965.25
99.3
5184.60
103.1
Iron
2081.0
2020.65
97.1
10000.0
10127.53
101.3
10309.26
103 . 1
Lead
100.0
102.80
102.8
50.0
49 .60
99.2
50.60
101.?
Magnesium
25700.0
24079.19
93.7
25000.0
24854.29
99 . 4
25265.50
101. ¦
Manganese
504.0
490.88
97.4
5000.0
4763.76
95. 3
4924.18
98.1
Mercury
3.8
3.58
94.2
5.0
5.29
105.8
5. 52
110.4]
Nickel
485.0
513.92
106.0
5000.0
5095.53
101.9
5126.29
102= 1
Potassium
10000.0
10200.00
102.0
10000.0
10340.00
103 . 4
10150.00
101. ¦
Selenium
100. 0
102.00
102.0
50.0.
48 . 40
96.8
48.50
97.1
Silver
484.0
479.85
99.1
1000.0
978.55
97.9
1019.75
102.0 1
Sodium
51500.0
50799.25
98.6
50000.0
49302.05
98 . 6
50706.66
101. fa1
Thallium
50.0
50.40
100.8
25.0
23 .40
93 . 6
23 . 30
93.1
Vanadium
505.0
505.93
100.2
5000.0
4898.40
98.0
5123.95
102.P
Zinc
2920.0
2910.56
99.7
5000.0
4916.53
98.3
4941.65
98.8
Cyanide
















I
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-llfl
FORM II (PART 1) - IN

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D414
Initial Calibration Source:	EMSL-LV,NBS_
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial
True
Calibration
Found %R (1)
True
Continuing Calibration
Found %R(1) Found
%R(1)

M
Aluminum



10000.0
10652.92
106.5
10237.74
102.4

P
Antimony_
Arsenic



5000.0
5055.10
101.1
5160.60
103.2

P
100.0

101.90
101.9
50.0
49.10
98.2
47. 60
95.2

F
Barium




2500.0
2524.68
101.0
2522.84
100.9

P
Beryllium
Cadmium



500.0
513.72
102.7
516.08
103.2

P



2500.0
2473.82
99.0
2482.17
99.3

P
Calcium



25000.0
26219.72
104.9
24943.74
99.8

P
Chromium



5000.0
4975.71
99.5
5000.97
100.0

P
Cobalt



5000.0
5056.65
101.1
5066.08
101.3

P
Copper



5000.0
5185.42
103.7
5215.50
104.3

P
Iron



10000.0
10594.51
105.9
10000.42
100.0

P
Lead



50.0
50.50
101.0
50.10
100.2

F
Magnesium



25000.0
26073.02
104 .3
25212.36
100.8

P
Manganese



5000.0
4939.94
98.8
4995.79
99.9

P
Mercury	
Nickel



5.0
4.94
98.8



AV



5000.0
5304.39
106. 1
5065.60
101. 3

P
Potassium



10000.0
10060.00
100.6
10100.00
101.0

A
Selenium



50.0
48.20
96.4
47.20
94.4

F
Silver



1000.0
1018.51
101.9
1022.76
102.3

P
Sodium



50000.0
51883.47
103.8
51828.62
103.7

P
Thallium



25.0
23.20
92.8
24.00
96.0

F
Vanadium



5000.0
5144.56
102.9
5185.88
103.7

P
Zinc



5000.0
4994.10
99.9
4996.24
99.9

P
Cyanide









NR











(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
7/87

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC	Case No. :MCFARLAND SAS No.: 	 SDG No.: It
Initial Calibration Source: EMSL-LV,NBS
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial Calibration
True Found %R(1)
Continuing Calibration
True Found %R(1) Found %R(®
Aluminum_
Antimony_
Arsenic	
Barium_i	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron



















50.0
	48.70
_97 . 4
































































Lead
	100.0
	95.60
_95. 6
50.0
	50.50
101. 0
	49.60
_99 . 2
Magnesium
Manganese
Mercury	
Nickel_i	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc




























o o
o o
o m
o
o
f—1
1
9980.00
	49.30
99.8
_98 . 6


100.0
	100.90
100.9
	49.60
_99«










50.0
	48.80
_97. 6
25.0
	24.50
_98 . 0
	25.70
102 ¦










Cyanide	
















(l) Control Limits: Mercury 80-120? Other Metals 90-110; Cyanide 85-m
FORM II (PART 1) - IN
7/8

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC	
Lab Code: LESC		Case No.: MCFARLAND SAS No.:
Initial Calibration Source: EMSL-LV,NBS_
Continuing Calibration Source: INTERNAL	
Contract: 68-03-3249
SDG No.: D414
Concentration Units: ug/L
Analyte
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron	
Lead
Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc
Cyamde_
Initial Calibration
True Found %R(1)
100.0
10000.0
108.70
9860.00
108.7
98.6
Continuing Calibration
True Found %R(1) Found %R(1)
50.0
50.0
10000.0
50.0
25.0
49.60
47.80
9860.00
49.10
26.00
99. 2
95.6
98.6
'98.2
104.0
47. 60
46.60
9760.00
48.40
24.80
95.2
93.2
97.6
"96.8
99.2
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
7/87

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.:
Initial Calibration Source:	EMSL-LV,NBS_
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial Calibration
True Found %R(1)
Continuing Calibration
True Found %R(1) Found %R(^
Aluminum_
Antimony_
Arsenic	
Barium	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron



















50.0
	51.00
102.0
	47.60
_9 5 .T











!
















































Lead
	100.0
97.80
_97.8
50.0
	51.30
102.6
	54.00
103^
Magnesium
Manganese
Mercury		
Nickel	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc





























_10000.0
_9620.00
_96 . 2
_9690.00












































Cyanide	
















(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-1]®
FORM II (PART 1) - IN

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC	Case No. :MCFARLAND SAS No.: 	 SDG No.: D414
Initial Calibration Source: EMSL-LV,NBS
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial Calibration
True Found %R(1)
True
Continuing Calibration
Found %R(1) Found
%R(1)

M
Aluminum


-






NR
Antimony_
Arsenic









NR
100.0
105.80
105.8
50.0
50.50
101.0
52.00
104.0

F
Barium









NR
Beryllium
Cadmium









NR









NR
Calcium









NR
Chromium









NR
Cobalt









NR
CoDDer









NR
Iron









NR
Lead



50.0
52.40
104.8
54.30
108.6

F
Magnesium









NR
Manganese









NR
Mercury	
Nickel









NR









NR
Potassium



10000.0
9580.00
95.8



A
Selenium









NR
Silver









NR
Sodium









NR
Thallium









NR
Vanadium









NR
Zinc



•





NR
Cyanide	









NR










(1) Control Limits: Mercury 80-120; other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
7/87

-------
"U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC	Case No.: MCFARLAND SAS No.: 	 SDG No.: II
Initial Calibration Source: EMSL-LV,NBS
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial Calibration
True Found %R(1)
Continuing Calibration
True Found %R(1) Found %R(^
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron







100 j







	100.0
	103.70
103.7
50.0
	49.4 0
_98 .8
	50.10





















































Lead
100.0
	93.20
_93 .2
50.0
	48.50
_97 .0
	49.10
_98^|
Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc


















































































Cyanide	
















(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 8 5-1]®
FORM II (PART 1) - IN

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No. :MCFARLAND SAS No.: 	 SDG No.: D414
Initial Calibration Source: EMSL-LV,NBS_
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial Calibration
True Found %R(1)
True
Continuing Calibration
Found %R(1) Found
%R(1)

M
Aluminum









NR
Antimony_
Arsenic









NR









NR
Barium









NR
Beryllium
Cadmium









NR









NR
Calcium









NR
Chromium"









NR
Cobalt









NR
Coooer









NR
Iron









NR
Lead



50.0
49.10
98.2



F
Magnesium









NR
Manganese









NR
Mercury
Nickel









NR









NR
Potassium









NR
Selenium

%







NR
Silver









NR
Sodium









NR
Thallium









NR
Vanadium



«





NR
Zinc









NR
Cyanide









NR











(1) Control Limits: Mercury 80-120; other Metals 90-110? Cyanide 85-115
FORM II (PART 1) - IN
7/87

-------
• U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEEDJESC	
Lab Code: LESC		Case No.:MCFARLAND SAS No.:
Initial Calibration Source: EMSL-LV,NBS_
Continuing Calibration Source: INTERNAL	
Contract: 68-03-3249
SDG No.:
Concentration Units: ug/L
Analyte
Initial Calibration
True Found %R(1)
Continuing Calibration
True Found %R(1) Found %R(1)
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron































































100.g





















Lead
	100.0
	101.50
101.5
50.0
	50.80
101.6
	50.30
Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc














































































Cyanide	
















(1)
Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-ll^|
FORM II (PART 1) - IN

-------
U.S. EPA - CLP
2A
INITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No. :MCFARLAND SAS No.: 	 SDG No.: D414
Initial Calibration Source: EMSL-LV,NBS_
Continuing Calibration Source: INTERNAL	
Concentration Units: ug/L
Analyte
Initial Calibration
True Found %R(1)
True
Continuing Calibration
Found %R(1) Found
%R (1)

M
Aluminum









NR
Antimony_
Arsenic









NR









NR
Barium









NR
Beryllium
Cadmium









NR









NR
Calcium









NR
Chromium









NR
Cobalt









NR
CoDDer









NR
Iron









NR
Lead
100.0
100.70
100.7
50.0
48.40
96.8
49.20
98.4

F
Magnesium









NR
Manganese









NR
Mercury
Nickel









NR









NR
Potassium









NR
Selenium









NR
Silver









NR
Sodium









NR
Thallium









NR
Vanadium









NR
Zinc
-








NR
Cyanide









NR











(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
7/87

-------
U.S. EPA - CLP
2B
CRDL STANDARD FOR AA AND ICP
Lab Name: LOCKHEED ESC	Contract: 68—03—3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: dP «•
AA CRDL Standard Source: INTERNAL	
ICP CRDL Standard Source: INTERNAL	
Concentration Units: ug/L
Analyte
Aluminum_
Antimony_
Arsenic	
Barium	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron	
Lead
Magnesium
Manganese
Mercury
Nickel^	
Potassium
Selenium_
silver	
Sodium	
Thallium_
Vanadium_
Zinc
CRDL Standard for AA
True
Found
%R






	10.0
9.20
	92.0






















5.0
4.20
	84.0











o o
• •
o in
o
o
in
1
4880.00
5.20
97. 6
_104.0





	10.0
8.90
	89.0







True
CRDL Standard for ICP
Initial	Final
Found %R	Found
I
400.0
	120.0
404.36
	119.78
101. 1
_99.8
435.55
	112.91
200.0
10.0
10.0
10000.0
20.0
100.0
50.0
	200.0
201.77
10.21
100.9
102.1
88.6
102. 0
107.9
109.4
95.2
_99.1
206.79
11. 08
8.86
4.72
10202.89
21.58
10578.04
19.26
109.44
47.61
96.80
50.07
	198.28
	251.75
10000.0
	30.0
9865.84
28.64
98.7
_95. 5
10431.58
29.26


	80.0
91.68
114.6
82.37






20.0
10000.0
21.86
109. 3
104 . 2
21.46
_10421.28
_10865.72
100.0
	40.0
105.19
40.26
105.2
100.6
109.03
46.14


FORM II (PART 2) - IN
7/87

-------
U.S. EPA - CLP
2B
CRDL STANDARD FOR AA AND ICP
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC	Case No.: MCFARLAND SAS No.: 	 SDG No.: D414
AA CRDL Standard Source: INTERNAL
ICP CRDL Standard Source: INTERNAL
Concentration Units: ug/L
Analyte
CRDL Standard for AA
True Found %R

CRDL Standard for ICP
Initial Final
True Found %R Found %R
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron
















	10.0
10.40
_104.0



































































Lead
5.0
5.00
_100.0





Magnesium
Manganese
Mercury	
Nickel
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc































5000.0
5.0
4580.00
4.70
91.6
	94.0

























	10.0
9.60
	96.0




























FORM II (PART 2) - IN
787

-------
•U.S. EPA - CLP
2B
CRDL STANDARD FOR AA AND ICP
Lab Name: LOCKHEEDJESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.:
AA CRDL Standard Source: INTERNAL	
ICP CRDL Standard Source: INTERNAL
Concentration Units: ug/L
Analyte
CRDL Standard for AA
True Found %R
CRDL Standard for ICP
Initial Final
True Found %R Found
Alummum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron














	10.0
9.70
	97.0


























































Lead
5.0
5.80
_116.0




Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc




















































































FORM II (PART 2) - IN
7/b;

-------
U.S. EPA - CLP
23
CRDL STANDARD FOR AA AND ICP
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D414
AA CRDL Standard Source: INTERNAL
ICP CRDL Standard Source: INTERNAL
Concentration Units: ug/L
Analyte
CRDL standard for AA
True Found %R
CRDL Standard for ICP
Initial Final
True Found %R Found %R
Alummum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium
Chromium_
Cobalt	
Copper	
Iron
















	10.0
8.70
	87.0



































































Lead
5.0
5.40
_108.0





Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc
































































































FORM II (PART 2) - IN
7/87

-------
"U.S. EPA - CLP
2B
CRDL STANDARD FOR AA AND ICP
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC	Case No.: MCFARLAND SAS No.: 	 SDG No.: 9
AA CRDL Standard Source: INTERNAL
ICP CRDL Standard Source: INTERNAL
Concentration Units: ug/L

CRDL Standard for AA

CRDL Standard for ICP




Initial
Final
Analyte
True
Found
%R

True
Found
%R
Found
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium
Chromium^
Cobalt	~
Copper	
Iron















	10.0
9.20
	92.0


























































Lead
5.0
4.60
	92 . 0




Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc




















































































FORM II (PART 2) - IN
7/87

-------
U.S. EPA - CLP
2B
CRDL STANDARD FOR AA AND ICP
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D414
AA CRDL Standard Source: INTERNAL
ICP CRDL Standard Source: INTERNAL
Concentration Units: ug/L
Analyte
CRDL Standard for AA
True Found %R

CRDL Standard for ICP
Initial Final
True Found %R Found %R
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium
Calcium
Chromium_
Cobalt	
copper	
Iron
























































































Lead
	5.0
4.30
	86.0





Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium^
Silver	~
Sodium
Thallium^
Vanadium"
Zinc










































































•




















FORM II (PART 2) - IN
7/87

-------
U.S. EPA - CLP
3
BLANKS
Lab Name: LOCKHEED ESC 		Contract: 68-~03—3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D4#
Preparation Blank Matrix (soil/water): SOIL_
Preparation Blank Concentration Units (ug/L or mg/kg): MG/KG
Analyte
Initial
Calib.
Blank
(ug/L)
C
Continuing Calibration
Blank (ug/L)
1 C 2 C 3
C

Prepa-
ration
Blank 1

Aluminum
40.0
U
57.2
B
69.6
B
40.0
V

15.619

Antimony_
60.0
U
60.0
U
60.0
U
60.0
u

17.215.

Arsenic
2.0
U
2.0
u

U



0 . 4 0 01
Ft
Barium
10.0
U
10.0
u
10.0
10.0
u

2.0001

Beryllium
1.5
U
1.5
u
1.5
U
1.5
u

0.300

Cadmium
4.0
U
4.0
u
4.0
U
4.0
u

0.800,

Calcium
25.0
U
68.3
B
106.6
B
25.0
u

5.000|
I--
Chromium
4.0
U
4.0
U
4.0
U
4.0
u

1.14 2*

Cobalt
13.0
U
14.3
B
13.0
u
13.0
u

2.600
u
Copper_
6.0
U
6.0
U
6.0
u
6.0
u

1.200|

Iron
12.0
U
45.4
B
92.0
B
14.7
B

22.6181

Lead
2.0
U
2.0
U
2.0
U
2.0
U

0.8001

Magnesium
129.1
B
195.6
B
256.8
B
155.6
B

33 .583
B
Manganese
3.0
U
3.0
U
3.0
U
3.0
u

0.6001

Mercury
0.2
U
0.2
U
0.2
U
0.2
u

0. 1501

Nickel
14.0
B
12.4
B
29.3
B
12.0
u

2.554

Potassium
300.0
U
300.0
U
300.0
U
300.0
u

60.000
u
Selenium
2.0
U
2.0
U
2.0
U
2.0
u

0 .4001

Silver
5.0
U
5.0
U
5.0
u
9.6
B

1.000J

Sodium
65.0
U
65.0
U
65.0
u
65.0
U

13.000

Thallium
2.0
U
2.0
U
2.0
u
2.0
U

0.400
u
Vanadium
14.0
U
14.0
U
14.0
u
14.0
U

2.800j
It
Zinc
11.5
B
11.6
B
10.0
u
10.0
U

2.000|

Cyanide























FORM III - IN
I/O

-------
U.S. EPA - CLP
3
BLANKS
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No. : MCFARLAND SAS No.: 	 SDG No.: D414
Preparation Blank Matrix (soil/water): 	
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
Initial
Calib.
Blank
(ug/L)
C
Continuing Calibration
Blank (ug/L)
1 C 2 C
3
C

Prepa-
ration
Blank
C

M
Aluminum


40.0
U








P
Antimony_
Arsenic


60.0
u

u






P
2.0
U
2.0
u
2.0






F
Barium


10.0
u








P
Beryllium
Cadmium


1.5
u








P


4.0
u








P
Calcium


25.0
u








P
Chromium


4.0
u








P
Cobalt


13.0
u








P
CoDoer


6.8
B








P
Iron

U
12.0
u

u

U




P
Lead
2.0
2.0
u
2.0
2.0




F
Magnesium


131.2
B








P
Manganese


3.0
u








P
Mercury



u








NR
Nickel


12.0








P
Potassium

U
300.0
u

u

U




A
Selenium
2.0
2.0
u
2.0
2.0




F
Silver


5.0
u








P
Sodium


65.0
u



U




P
Thallium
2.0

2.0
u
2.0

2.0




F
Vanadium


14.0
u








P
Zinc —


10.0
u








P
Cyanide












NR














FORM III - IN
7/87

-------
U.S. EPA - CLP
3
BLANKS
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.: 	 SDG No.:
Preparation Blank Matrix (soil/water): 	
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
Initial
Calib.
Blank
(ug/L)
C
Continuing Calibration
Blank (ug/L)
1 C 2 C 3
c

1
Prepa-
ration 1
Blank £l
Aluminum











Antimony_
Arsenic

u





u


1
2.0
2.0
u
2.0
u
2.0


1
Barium











Beryllium
Cadmium






















Calcium











Chromium











Cobalt










I
Copper










1
Iron

u





u



Lead
2.0
2.0
u
2.0
u
2.0



Magnesium











Manganese











Mercury	
Nickel






















Potassium
300.0
u
300.0
U
300.0
u
300.0
u



Selenium











Silver











Sodium











Thallium











Vanadium











Zinc











Cyanide	


















_



FORM III - IN
7/r.

-------
U.S. EPA - CLP
3
BLANKS
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
,ab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D414
Preparation Blank Matrix (soil/water): 	
'reparation Blank Concentration Units (ug/L or mg/kg): 	
Analyte
Initial
Calib.
Blank
(ug/L)
C
Continuing Calibration
Blank (ug/L)
1 C 2 C 3
c

Prepa-
ration
Blank
C

M
Aluminum












NR
Antimony_
Arsenic ~












NR


l
o
•
fM
u








F
Barium












NR
Beryllium
Cadmium












NR












NR
Calcium












NR
Chromium












NR
Cobalt












NR
CoDDer












NR
Iron



u








NR
Lead


2.0
1
o
•
CM
u






F
Magnesium












NR
Manganese












NR
Mercury	
Nickel












NR












NR
Potassium


300.0
u








A
Selenium












NR
Silver












NR
Sodium












NR
Thallium












NR
Vanadium












NR
Zinc












NR
Cyanide












NR











_l
1	
FORM III - IN
7/87

-------
¦ U.S. EPA - CLP
3
BLANKS
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	 SDG No.: 1^|.
Preparation Blank Matrix (soil/water): 	
Preparation Blank Concentration Units (ug/L or mg/kg): 	
Analyte
Initial
Calib.
Blank
(ug/L) C
Continuing Calibration
Blank (ug/L)
1 C 2 C 3 C
Prepa-
ration
Blank
1
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron

U
U

U
U

—

—







2.0
2.0











































Lead
2.0
2.0



Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc























































Cyanide	











FORM III - IN
7/8 /

-------
U.S. EPA - CLP
3
BLANKS
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC	Case No.:MCFARLAND SAS No.: 	 SDG No.: D414
Preparation Blank Matrix (soil/water): 	
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
Initial
Calib.
Blank
(ug/L)
c
Continuing Calibration
Blank (ug/L)
1 c 2 C 3
c

Prepa-
ration
Blank
C

M
Aluminum












NR
Antimony_
Arsenic












NR












NR
Barium












NR
Beryllium
Cadmium












NR












NR
Calcium












NR
Chromium












NR
Cobalt












NR
CoDoer












NR
Iron

u

u








NR
Lead
2.0
2.0








F
Magnesium












NR
Manganese












NR
Mercury	
Nickel












NR












NR
Potassium












NR
Selenium












NR
Silver












NR
Sodium












NR
Thallium












NR
Vanadium












NR
Zinc












NR
Cyanide	












NR












FORM III - IN
7/87

-------
U.S. EPA - CLP
ICP INTERFERENCE CHECK SAMPLE
Lab Name: LOCKHEED_ESC	
Lab Code: LESC		Case No.:MCFARLAND SAS No: 	
ICP ID Number: PLASMAII		ICS i'ource: UNLV
Contract: 68-03-3249
	 SDG No.:
Concentration Units: ug/L
Analyte
True
Sol. Sol.
A	AB
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron	
Lead
Magnesium
Manganese
Mercury	
Nickel
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc	
498000
0
	0
	0
	0
468000
	0
	0
0
188000
463000
0
483000
0
	461
	452
	875
457000
I	466
	438
454
182000
447000
475
898
1010
0
4 68
"958
Initial Found
Sol.	sol.
A	AB	%R
553587
21
	9
	1
-5
491149
|	39
	14
5
212121
502389
21
20
	4
¦44
19
13
542446.2
1.3
420.7
433.4
838.2
465.1
421.7
471.1
208572.0
504955.0
438.5
909.3
911.7
6.3
473.4
'897.9
112.3
_S 1.3
_? 5.9
_«¦ 5.8
lCl.9
_9>. . 8
_9i .3
1(' .8
ll£.6
TiTTo
92.3
102 . 3
9C . 3
101.2
93.7
Final Found
Sol.	Sol.
A	AB
550860
-53
	8
	0
-11
486455
I	39
	10
	8
208892
506104
"	22
17
_1
15
14
'16
544916.1
"	22.3
		449.8
	469.3
	851.2
488364.1
[	491.0
	447.8
512.4
207388.7
501385.9
462.3
886.5
968.2
"-10. 3
493 . 1
'934 . 2
97,
112
97
I
FORM IV - IN

-------
U.S. EPA - CLP
5A
SPIKE SAMPLE RECOVERY
Lab Name: LOCKHEED_ESC		 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): SOIL_
EPA SAMPLE NO,
M510
SDG No.: D414
Level (low/med):
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Analyte
Aluminum_
Antimony_
Arsenic	
Bariumn	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	~
Copper	
Iron	
Lead
Magnesium
Manganese
Mercury	
Nickel
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc
Cyanide
Control
Limit
%R
75-125
75-125"
75-125"
75-125"
75-125"
75-125
75-125"
75-125"
75-125
75-125
75-125"
75-125"
75-125
75-125"
75-125
75-125"
75-125"
Spiked Sample
Result (SSR)
9376
;	58
	10
	4 81
	10
8
3403
1_405
	106
63
13074
I	19
_3774
	360
0
110
.0000
.4000"
.0000"
.7000"
.4000"
.8000"
.5000"
.3000"
.5000"
.5000"
.5000"
.2000"
.9000"
.2000"
.8000"
.8000"
	1.9000
	93.8000"
349.0000"
1_10.1000"
125.8000"
'160.0000"
B
Sample

Spike



Result (SR)
C
Added (SA)
%R
Q
M
8489.7000




NR
12.6000
0
105.2
55.5
N
P
1.9000
B
8.4
96.4

F
96.6000
U
420.6
91.6
~
P
0.3000
10.5
99.0
~
P
0.8000
u
10.5
83.8

P
3320.3000




NR
12.9000
B
420.6
93 .3

P
6.1000
105.2
95.4

P
12.2000

52.6
97.5

P
13082.5000




NR
15.6000

4.2
85.7

F
3666.4000




NR
242.9000

105.2
111.5

P
0.1000
a
1.0
80.0

AV
9.5000

105.2
96.3

P





NR
0.4000
u
2.1
90.5

F
1.1000
u
105.2
89.2

P
380.1000
B



NR
0.5000
B
10.5
91.4

F
26.7000

105.2
94 .2

P
63.0000

105.2
92.2

P





NR






Comments:
FORM V (PART 1) - IN
7/87

-------
•U.S. EPA - CLP
5B
POST DIGEST SPIKE SAMPLE RECOVERY
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
EPA SAMPLE
M510
SDG NO. : D4I
Matrix (soil/water): S0IL_
Level (low/med): 		
Concentration Units: ug/L
Analyte
Control
Limit
%R
Spiked Sample
Result (SSR) C
Sample
Result (SR) C
Spike
Added (SA)
%R
Aluminum_
Antimony^
Arsenic ~
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron


—

U



465.40
60.00
500.0
	93.1









•


































Lead





Magnesium
Manganese
Mercury	
Nickel
Potassium
Selenium_
Silver	~
Sodium	
Thallium_
Vanadium_
Zinc





	
















































Cyanide	










Comments:
FORM V (PART 2) - IN

-------
U.S. EPA - CLP
DUPLICATES
EPA SAMPLE NO.
Contract: 68-03-3249
"ab Name: LOCKHEED_ESC	
ijab Code: LESC		Case No.: MCFARLAND SAS No.:
atrix (soil/water): SOIL_
* Solids for Sample: _95.l
M510 D
SOG No.: D414
Level (low/med):
% Solids for Duplicate: _95.1
Concentration Units (ug/L or mg/kg dry weight): MG/KG
Analyte
Aluminum^
Antimony"
Arsenic	
Barium_i	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron	
Lead	
Magnesium
Manganese
Mercury
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc
Cyanide
Control
Limit

Sample (S)
C

Duplicate (D)
C

RPD

Q
M


8489.7500


8783.4100


3.4

~
P
12.6

12.6200
0

17.2700





P
2.1

1.9300
B

2.5700


28.4


F
42. 1

96.6000
U

105.7700


9.1

—
P
1.1

0.3200

0.3200
B



—
P
1.1

0.8400
u

0.8400
U




P
1051.5

3320.2600


3469.8800


4.4


P


12.8900


13.7600


6.5


P
10.5

6.0800
B

6.9700
B

13.6

~
P
5.3

12.2300


15.5900


24.2


P


13082.4900


11816.9500


10.2


P


15.6500


14.0400


10.8

~
F
1051.5

3666.4200


3723.5800


1.5"


P


242.8500


253.8100


4.4


P
0.1

0.1400
U

0.1400
U




AV
8.4

9.5300


7.7300
B

20.9


P
1051.5

3819.1400
U

3735.0200


2.2


A
1.1

0.4200

0.4200
U




F
2.1

1.0500
U

1.2500
B




P
1051.5

380.1400
B

402.0000
B

5.6


P
2.1

0.4600
B

0.4200
U




F
10.5

26.7200


26.6400


0.3


P


63.0300


64.5300


2.4


P











NR












FORM VI - IN
7/87

-------
U.S. EPA - CLP
7
LABORATORY CONTROL SAMPLE
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.:
Solid LCS Source: QB2S86	
Aqueous LCS Source: 	
Analyte
Aqueous (ug/L)
True Found %R
Solid (mg/kcf)
True Found C Limits
Aluminum_
Antimony_
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron



_15802.0
_12756.2
—
	9711.0
21894.0






17.0
13.8
8.0
26.0



	260.5
	235.2
	205.0
	316.0






11.5
9.0
8.0
15.0



2826.0
41.0
2446.1
35.4
66.4
21.5
1900.0
28.0
3756.0
54.0






78.5
54.0
103.0
37.0



25.5
14.0



20850.0
33.0
17947.9
27.0
15764.0
11.0
25937.0
55.0
Lead



Magnesium
Manganese
Mercury
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
vanadium_
Zinc



4908.0
367.5
18.0
4008.7
314.3
20.2
3817.0
311. 0
5.0
6000.0
424 . 0
31.0









31.0
29.9
22.0
40.0



2985.0
24.5
2228.0
20.5
1900.0
17. 0
4070.0
32 . 0






25.5
23.1
21.0
30.0

















65.5
57.0
49. 0
82.0



54.0
45.7
40.0
68. 0
Cyanide	














O
18
»7
FORM VII - IN
7/^7

-------
U.S. EPA - CLP
8
STANDARD ADDITION RESULTS
Lab Name: LOCKHEED_ISC		Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.:	SDG No.: D414
Concentration Units: ug/L
EPA
Sample
No.
An
oil.
0 ADD
Abs -
1 ADD
CON ABS
2 ADD
CON ABS
3 ADD
CON ABS
Final
Cone.
r
P803
D414
F1204
LS13
M510 0
N116	
AS
PB
PB
PB
PB
PB
l
l
n
l
l
7
8.400
30.000
""40.700
"38.500
"67.200
21.200
18
20
20
20
20
20
27.400
48.800
"61.500
""57.400
"87.100
39.800
36
"39
"39
"39
"39
_39
45.600
"68.900
80.100
"76.100
108.800
58.500
54
"59
59
59
59
59
63.600
90.400
102.700
97.800
T31.200
80.900
9.4
0.9999
0.9993
0.9992
0.9991
0.9994
0.9986
31.2
424.7
41.4
66.8
132.4






















,—






























—





























































—



















*
—

















































FORM VIII - IN
7/87

-------
U.S. EPA - CLP
9
ICP SERIAL DILUTION
Lab Name: LOCKHEED_ESC	 Contract: 68-03-3249
Lab Code: LESC		Case No.:MCFARLAND SAS No.: 	
Matrix (soil/water): S0IL_
EPA SAMPLE
M510
SDG No. : D|
Level (low/med): 	
Concentration Units: ug/L
Analyte
Aluminum^
Antimony_
Arsenic ~
Barium^	
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron	
Lead	
Magnesium
Manganese
Mercury	
Nickel^	
Potassium
Selenium_
Silver	
Sodium	
Thallium_
Vanadium_
Zinc	
Initial Sample
Result (I) c
40368.70
60.00"
459.30
^	1.50"
4.00"
15787.90
*	61.30'
	28.90"
58.20"
62207.20
17433.80
1154.80"
45.30
	5.00
1807.60"
127.00
*299.70"
U
B
Serial


I
Dilution


Differ-
Result (S)
c

ence
42637.00
U

5.6
300.00



B


532.10

15.9
7.50
U


20.00
U


16701.20
B

5.8
67.70
U

10.4
65.00


63 .90
B

9.8
65574.40
—

	5.4_
18546.20
B

6.4
1244.20
—

	7 .7_
78.10
B

	72.4_

U


25.00


1641.30
B

	9 . 2_
167.50
B

31.9
359.80
—

	20.1_

Q
M

—
P~


NR


F


P


NR


NR


P


P


NR


P


P


F


P


P


F


P


AV


F


NR


P


F


P

—
P
FORM IX - IN
7f

-------
U.S. EPA - CLP
10
HOLDING TIMES
Lab Name: LOCKHEED ESC	Contract? 68—03—3249
Lab Code: LESC_	Case No.:MCFARLAND SAS No.: 	 SDG No.: D414
EPA

Date
Sample No.
Matrix
Received
D414
SOIL
07/25/89
D802
SOIL
07/25/89
DF01
SOIL 	
07/25/89
F1204
SOIL
07/25/89
H709
SOIL
07/25/89
11205
SOIL
07/25/89
J212
SOIL
07/25/89
K411
SOIL
07/25/89
L4A07
SOIL
07/25/89
L513
SOIL
07/25/89
M14A08
SOIL
07/25/89
M4A06
SOIL
07/25/89
M510
SOIL
07/25/89
M510 D
SOIL
07/25/89
M510 S
SOIL
07/25/89
N116
SOIL
07/25/89
P715
SOIL
07/25/89
P803
SOIL
07/25/89
R1417
SOIL
07/25/89















Mercury
Prep
Date
08/17/89
'08/17/89
"08/17/89
"08/17/89
"08/17/89
"08/17/89
"08/17/89
'08/17/89
"08/17/89
"08/17/89
"08/17/89
"08/17/89
"08/17/89
"08/17/89
'08/17/89
"08/17/89
"08/17/89
"08/17/89
"08/17/89
Mercury
Holding
Tine
23
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
"23"
Cyanide
Prep
Date
Cyanide
Holding
Time
FORM X - IN
7/87

-------
U.S. EPA - CLP
11
INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LOCKHEED_ESC		Contract:
Lab Code: LESC	Case No.:MCFARLAND SAS No.:
ICP ID Number:	PLASMAII		Date:
Flame AA ID Number : 	
Furnace AA ID Number :
Analyte
Wave-
length
(nm)
Back-
ground
CRDL
(ug/L)
IDL
(ug/L)
M
Aluminum
396.15

200
40.0
P
Antimony_
Arsenic
217.58

60
60.0
P


10

NR
Barium
455.43

200
10.0
P
Beryllium
cadmium
313.11

5
1.5
P
214.44

5
4.0
P
Calcium
422.67

5000
25.0
P
Chromium
267.72

10
4.0
P
Cobalt
228.62

50
13.0
P
Copper
324.75

25
6.0
P
Iron
238.20

100
12.0
P
Lead


5

NR
Magnes ium
202.85

5000
90.0
P
Manganese
257.61

15
3.0
P
Mercury	
Nickel


0.2

NR
231.60

40
12.0
P
Potassium


5000

NR
Selenium


5

NR
Silver
328.07

10
5.0
P
Sodium
589.59

5000
65.0
P
Thallium


10

NR
Vanadium
294.40

50
14.0
P
Zinc
213.86

20
10.0
P






Comments:
68-03-3249
	 SDG No.: Dj-
02/10/89
FORM XI - IN

-------
U.S. EPA - CLP
11
INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D414
ICP ID Number:			Date: 02/10/89
Flame AA ID Number : FIAAV	
Furnace AA ID Number : PE5100	
Analyte
Wave-
length
(nm)
Back-
ground
CRDL
(ug/L)
IDL
(ug/L)
Aluminum_
Antimony_
Arsenic ~
Barium
Beryllium
Cadmium
Calcium
Chromium_
Cobalt	~
Copper	
Iron


200



60

_193 .78
	BZ	
10
2.0
200
5"






5



5000
10"






50



25



100

Lead
_283.38
	BZ	
5
2.0
Magnesium
Manganese
Mercury	
Nickel
Potassium
Selenium
Silver	
Sodium	
Thallium_
Vanadium_
Zinc
5000
15"




_253.78

0.2
0.2

40



5000
5

__196.08
	BZ	
2.0
10



5000
10"

_276.88
	BZ	
2.0
50



20






M
NR
NR
F_
NR
NR
NR
NR
NR
NR
NR
NR
F__
NR
NR
AV
NR
NR
F
NR
NR
F_
NR
NR
Comments:
FORM XI - IN
7/87

-------
• U.S. EPA - CLP
11
INSTRUMENT DETECTION LIMITS (QUARTERLY)
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.:
ICP ID Number:			Date:	02/10/89
Flame AA ID Number : PE5100F	
Furnace AA ID Number :
Analyte
Wave-
length
(nm)
Aluminum^
Antimony"
Arsenic	
Barium^	
Beryllium
Cadmium	
Calcium
Chromium
Cobalt	
Copper	
Iron











Lead

Magnesium
Manganese
Mercury
Nickel^	
Potassium
Selenium
Silver	
Sodium	
Thallium
Vanadium"
Zinc













Back-
ground
CRDL
(ug/L)
200
~_60'
_1°~
200"
"	5"
5"
5000
|	10"
	50"
	25"
__100"
5"
5000
;	is"
	0.2"
	40"
5000"
"	5"
	10"
5000"
10"
	50"
20"
IDL
(ug/L)
300.0
M
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
A
NR
NR
NR
NR
NR
NR
Comments:
FORM XI - IN
7/E

-------
U.S. EPA - CLP
12A
ICP INTERELEMENT CORRECTION FACTORS (QUARTERLY)
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D414.
ICP ID Number: PLASMAII		Date: 02/10/89
Analyte
Wave-
length
(nm)

Interelement Correction Factors for :
A1 Ca Fe Mg 	
Aluminum^
Antimony^
Arsenic	
Barium
Beryllium
Cadmium	
Calcium	
Chromium_
Cobalt	
Copper	
Iron
396.15
~217.58_





J).3000000








455.43
JS13.11_
214 * 44
422.67"
267.72
228.62
324.75"
238.20"
220.55
"202.85"
"257.61_










-0.0400000




























Lead
-0.2000000




Magnesium
Manganese
Mercury
Nickel^	
Potassium
Selenium_
Silver	
Sodium
Thallium^
Vanadium^
Zinc














231.60
_766.49~















328.07
_589.59_















294.40
_213.86"







_0.1000000

_0.0000000




Comments:
FORM XII (PART 1) - IN
7/87

-------
U.S. EPA - CLP
13
ICP LINEAR RANGES (QUARTERLY)
Lab Name: LOCKHEED_ESC		Contract: 68-03-3249
Lab Code: LESC		Case No.: MCFARLAND SAS No.: 	 SDG No.: D4i
ICP ID Number: PLASMAII		Date:	02/10/89
Analyte
Integ.
Time
(Sec.)
Concentration
(ug/L)
M
Aluminum
3 .00
150000.0

Antimony_
Arsenic
3 .00
10000.0



NR
Barium
7.00
35000.0

Beryllium
Cadmium
1.00
20000.0

18.00
100000.0

Calcium
3.00
600000.0

Chromium
18.00
500000.0

Cobalt
10.00
200000.0

Copper
11.00
250000.0

Iron
4.00
100000.0

Lead



Magnesium
3.00
600000.0

Manganese
4.00
150000.0

Mercury


NR
Nickel
10. 00
500000.0

Potassium
14.00
200000.0

Selenium


NR
Silver
9.00
750000.0

Sodium
3.00
300000.0

Thallium


NR
Vanadium
11.00
150000.0

Zinc
7.00
400000.0

•



Comments:
FORM XIII - IN

-------
Appendix 4
SEMI-VOLATILE CHEMICAL ANALYSES
McFarland, California
D1

-------
13
EPA SAMPLE NO.
SEMIVOLATILE ORGAWICS ANALYSIS DATA SHEET		
I
Lab Name: Lo&U.h ;= l?J — j~ £ C. Contract:^
Lab Code: 	
Case Ho.	SAS No.:
SOG No.:
Matrix: (soil/water) i>0 t L-
Sample wt/vol:	3&-C (Q/mL)
Level: (low/med) LC\aJ
% Moisture: not dec. C,l dec.
Lab Sample ID:	2.
Lab File ID: ^£.5^ 7"?
Extraction: (SepF/Cont/Sonc) 56
G?C Cleanup: (Y/N) V	pH:	
Date Received:
Date Extracted: 7 fly
Date Analyzed: thhl-
CAS NO.
COMPOUND
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or uq/Kq) UCr )
LA
108-9S-2	
—Phenol
111-44-4	
—bisf2-Cftloroethvl) ether
95-57-8	
—2-Chlorophenol
541-73-1	
—1.3-Dichlorobenzene
106-46-7	
—1.4-Dichlorobenzene
100-51-6	
—Benzvl alcohol
95-50-1	
—1.2-Dichlorobenzene
95-48-7	
—2-Methvloheno1
108-60-1	
—bis(2-Chloroisopropyi)etiier_
106-44-5	
—4-Methylphenol
621-64-7	
—N-Hitroso-di-n-propylamine	
67-72-1	
—Hexachloroethane
98-95-3	
—Nitrobenzene-
78-59—1	
—Isophorone
88-75-5	•	
—2-Hitrophenol
105-67-9	
—2.4-DimethvlDhenol
65-85-0	
—Benzoic acid
111-91-1	
—bis(2-Chloroethoxy)methane _
120-83-2	
—2.4-Dichloroohenol
120-82-1	
	1.2.4-Trichlorobenzene
91-20-3	
-—Naohthalene
106-47-8	
—4 -Chloroaniline
87-68-3	
—Hexachlorobutadiene
59-50-7	
	4-Chloro-3-methylohenol <*
91-i 7-6	
-—2-Methylnaphthalene
77-47-4	
-—Hexachlorocyclopentadiene_	
88-06-2	
	2 . i.6—Trichlorophenol
95-95-4	
	2 f 4.5-TrichloroDhenol
91-58-7	
	2-ChloronaDhthalene
38-74-4	
	2-Mitroaniline
131-11-3	
—Oimenhylphthalate 	
208-96-8	
—AcenaDhthylene
606-20-2	
-—2.6-Oinitrocoluene
MlCl
J^L
? -2.0 O

1 O
b 2.00 \
6 & I
i
FORM I SV-1
1/87 Rev.

-------
1C
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: U oc kh &!=<^Contract:65'3?~32	^
Lab Code: _______ Case No. :/2-L/5a.Ia*J SkS No.: 	
SDG No.:
Matrix: (soil/water) 
99-09-	2	
33-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
34-66-	2	
7005-72-3—
86-73-7	
100-01-	6	
524-52-1	
36-20-6	
101-55-	3	
113-74-1	
S7-86-5	
85-01-3	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
213-01-9	
117-31-7	
117-34-0	
205-99-2	
207-03-	9	
50-32-3	
193-39-5---
53-70-3	
191-24-2	
-3-Nitrcaniline_
-Acenaotithene
¦2,4-Dinitroptienol_
-4-Nitrophenol	~
-Dibenzofuran
¦2,4-Dinitrotoluene_
¦Diethylphthalate_
	4-Chloroptienyl-ptienylether	
——Fluorene	
	-4-Nitrcanilir.e
-4,6-Dinitro-2-metftylphenoi	
—M-Mitrosodiphenylamine (1)	
—4-3roacptienyl-ptienyletfier	
—Hexachlorobenzene
--Pentachlorcphenol	
—Phenanthrene		
—Anthracene
—Di-n-butylptithalate
—rluoranthene	
—Pyrene
-9utylbenzylptithalate	
-3,2 * -D. -.lorobenzidine
-9enzo (a . nttiracene
•Chrysene
—bis(2-Ethylnexyl)pntnalate._
—Qi-n-octylphthalate		
—Senzo(b)tluoranthene	
—5enzo(K) fluoranthene	
—3enzo(a)pvrene_
—Indeno(1,2,3-cd)pyrene_
—Oibenz(a,h)anchracene_
—Senzo(g,n,i;perylene	
1 2. £C, | U
0\
¦blao
^ZCCD1

A=-
4 s

2<£ C
i £ !

y ¦ 1
6 6 C

w 4*
/o t- C
13_&£\
/-6C\
as
<: ta 1 cj
(1) - Cannot be separaced ircm Dipnenyiamme
FORM I SV-2
1/87

-------
IF
SEMTVOLATILZ ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE HO,
Lab Name
Lab Cade
: L&Cj Contract:d&| J) f
: 	 Case No. iM.5d/*tJ SAS No.: 	 SCO No.: 	
Matrix: (soil/water) 50! L-
Saaple wt/vol:	30 (g/mL) 6-
Level: (low/ned) L0W
\ Moisture: not dec.	dec.	
Ixtraction: (SepF/Cont/Sonc) 5QA/C—
G?C Cleanup: (Y/H) £	PH:	
Lab Sample ID: ^ / 7 2-
Lab File ID:
Date Received: 7 / "2- *7
Date Extracted: _7/27/t;
Date Analyzed:
Dilution Factor:

Number TICs found:
CONCENTRATION UNITS: y
(ug/L or ug/Kq} jj6- /
CAS NUMBER

COMPOUND NAME
I
RT
EST. CONC.
i
tj *j ><£ »>a w Q
/ /go
l_2.
\_±JZ£
3 
-------
IB
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NC
Lab Name: Lack
I	I
^ ^ Contract:—721 	
Lab Code:
Case No. Aft.&AfontjSkS No.:
SDG No.
Matrix: (soil/water) i U
A
Sample vt/vol:	?C
-------
1C
SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Nam®: Lo&k. hgcJContract:1 ^
	 Case Mo.	SAS No.: 	
Lab Coda: 	
Matrix: (soil/water) 'rO!^
Sample vt/vol:	9^><3(q/mL) 0~~
Level: (low/mad) LCi M
% Moisture: not dec. *~f/ *^1 dec.		
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: CY/N) V	pH:	
SOG No.:
Lab Sample ID:	*"7
Lab File ID:
CAS NO.
COMPOUND
Date. Received: 7/3.5/99
Date Extracted:
~ate Analyzed: «? hch<7
Dilution Factor: / , O
CONCENTRATION UNITS; .
(ug/L or uq/Kq) U6~!t-3,3* -D. -ilorobenz idine
—Ben z o(a nthracene	
¦Chrysene
—bis(2-Ethylhexy1)pnthalate
—Di-n-octylphthalate_
—9enzo(b)fluoranthene
—aenzo(k)fluoranthene
—3enzo(a)pyrene	
—Indeno(1,2,3-cd)pyrene
—Oibenz(a,h)antftracene_'
—9enzo(g,h,i)perylene_





±±lqc

j^Li£
±


J2_2.

=kL
<146
t±Cl
3

•?" 2m
(i
(1) - Cannot be separated r'ron Oipnenylaame
jL

FORM I SV-2
1/87 Rev.

-------
IF
SEMIVOIATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NC
Lab Nana: L ac-khts&J - B	 Contract:: £$	f f | 3 $
Lab Code: _______ Case No.	SAS No.: _____
Matrix: (soil/water) £~
Saaple wt/vol:	1 O (t-'pCL -j
Date Received:
Date Extracted:
Date Analyzed: ^ Jltf/S'j
Dilution Factor: )* Cj
Huaber TICs found:
CONCENTRATION UNITS; .
(ug/L or ug/Kg) U/+-Iktf-
SST. CONC.
t / GO

/ 2 O C
% *~t 0 Ct
tLSjL
\w£L
l22S
/ R £o
2. OlS
\±3>tifLj<
£
CAS NUMBER
1.
2.
3.
«. ¦
5.
~7 c ' 4 H rf
6.
7.
8.
o.
10.
;c-*? ?_—r
11.
12.
13.
14.

15.

16.

17.

18.

19.

20.

21.

22.

23.

2 4 .

25.

26.

27 ,

28.

29.

20.
'
COMPOUND NAME

c/A/U*//*•*/«/ M	)0<2«s
(J */ «" l*<9		
I	£f* ei s* f jOt? l/
£/~A *me , /. /, z,X. • Trfi?
1/1'-' t-1 s>

fj
>J >/*

is 3? ^ f £r/*yC <
jS <*s a? +* si*
L/	iv a/

I is <* (4 h *> >.is«%/

O <\s « <*r	^ s> ¥1/f C-+A f I
Z.	^s,/y Aac*£ Vat/
FORM I SV-TIC
1/87

-------
13
SEMXVOLATXLZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name
Lab Code:
SLo&k Ins/zJ -E5^
Contract;
Case No.	J SAS No.:

SCG No.:
Matrix: (soil/water) *r/Q)L-
Sample vt/vol:	^0,0 (q/nL) 6~
Level: (lov/med) Lq
% Moisture: not dec. 2. (O dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N) Y	pH:	
CAS NO.
COMPOUND
Lab Sample ID: <73/5"?
Lab File ID:	3
Date Received: ~7
Date Extracted: ~7/"ZJn~
Date Analyzed: *5i2-?) /*%*?
Dilution Factor: / , &
CONCENTRATION UNITS:
(ug/L or uq/Kg) l)Q~ / fCa; q
108-95-2-
111-44-4	
95-57-8	
541-73-1—
106-46-7—
100-51-6—
95-50-1	
95-48-7	
108-60-1—
106-44-5—
621-64-7 —
67-72-1	
98-95-3	
78-^9-1	
88-75-5—
105-67-9-
65-85-0—
111-91-1-
120-83-2-
120-82-1-
91-20-3 —
106-47-8
87-68-3-
59-50-7-
91-i 7-6-
77-47-4-
88-06-2-
95-95-4-
91-58-7-
33-74-4 -
131-11-3
208-96-8
606-20-2
-——Phenol
¦bis(2-Chloroethyl)ether_
¦ 2-Chio ropheno1_
¦l,3-0ichlorobenzene_
¦1,4-Dichlorobenzene"
»3enzyl alcohol^
¦1,2-Dichlorobenzene_
¦ 2-Methylpheno1_
•bis(2-Chloroisopropyl)ether_
¦ 4-Methylpheno1
—N-Nitroso-di-n-propylamine	
—Hexachloroethane	
—Nitrobenzene	
—Isophorone
—-——2-M itropheno1_
—2,4 - Dimethy 1 pheno 1_
—Benzoic acid	
—bis (2-Chloroethoxy) metiiane	
—2,4-Dichlorophenol
—1,2,4-Trichlorobenzene_
- -Naphthalene_
——4-Chloroaniline	
———Hexachlorobutadiene
—4-Chloro-3-methylphenol_
—2-Methylnaphthalene_
Grro
— /
_U^L
~7
-------
1C
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO
Lab Name: b£F-d'Ez"^> contract | t / ^ ^
Lab Code: 		 Case So. -y'Je-feAltnJSA5 No.: ______ SDG No.: 	
Matrix: (soil/water) *7£! L
Sample vt/vol:	t£,Q (g/mL) &
Level: (low/med) LCu\/
% Moisture: not dec. 2 e& dec.	
(SepF/Cont/Sonc)
(Y/N) Y	cH:	
Lab Sample ID: c> f /h 9
Lab File 13:	?
Extraction:
Date. Received:
Date Extracted: "7/2 jr/g'*7
Date Analyzed: 5/2?/y?
Dilution "actsr: > >  ~70
-*cc?
¦4,6-Dinitro-2-aeti:ylpnenoi	
-N-Nitrosodiphenylamine (1)	
-4-Srcaophenyl-phenylether	
-Hexachlorobenzene
-Pentaccftlorcphenol	
-rhenanthrene	
-Anthracene
? "ICC*
—Di-n-butylphthalate
—Fluoranthene	
—Pyrene
-Sutylbenzylphthalate	
-3 , 3 ' -0. -.lorobenz idine
-3enzo(a nthracene	
Chrysene
is TO

G *7 &

Jul.
±

t-ro
—bis (2-Ethylhexyl) phtnalate	I
¦-Oi-n-octy'lphthalate	I
--3enzo(b) fluoranthene	_J
--5enzo(k) r'luoranthene	I
— Senzo (a) pyrene	 !
—Indeno(1,2.3-cd)pyrene	
—Oibenz(a,h)anthracene	
—3enzo(g,h,i)perylene	
It#
£ 7 £
(1) - Cannot be seoaracaa irsrr. oipnenylamine
J

Jj-
3
13

FORM I SV-2
1/37

-------
IF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name
t (-pcilhjzEd ^	Contract: & ^| F~ I ^
Lab Code:
Case No.
SAS No.
Matrix: (soil/water) J2&ZL
Sample vt/vol:	(q/aL)
Level: (low/med) LcD US
\ Moisture: not dec. "2 i 0 dec.	
Extraction: (SepF/Cont/Sonc) "?{)/)£
G?C Cleanup: (Y/N) V_	pH:	
SDG No.
Lab Sample ID:
Lab File ID:	V J
Date Received: 7 A 4-7^
Date Extracted: 1 J~2-b }3 ^
Date Analyzed: g/Wg?
Dilution Factor: / t &
Number TICs found: 2.*?
CONCENTRATION UNITS:. ^
(ug/L or uq/Xq) /J/r }KIT"

CAS NUMBER
1.
2.
3.
4 .
5.
6.
7 .
3.
o.
10.
11.
12.
13.
14.
15.
16.
17.
18.
19.
20.
21.
22.
23	.
24	.
25.
26.
27	.
28
29
20
rrK&r)
COMPOUND NAME
(J 4/ k? ,y ff t/
l/ a/ i,.
WZ.
		I tJ «/£*//>
r£b,l
C> SLA.1US a/		
I U 4/ £ .iff] lA/ A/"A fa?-*/
		I L//V	'S
'fat*
J4y4At> i
/ic*f*IOa ¦«/
1 U+/M ha us V MyJAa b,j i/

AA^s**- t~j r	
\t)*jK	* k)s A/
I 01	; mJn - £''', AJ-*/£

iH *6
Z.1 7
* too
7. 6 H
-LO&O
7,5 -»

-7. /
¦$*>/:¦
t-n
t is G6
•? .2*
n-XO

1 6/^

1 / 70 0
«f ./7
1
4.
I

1 7 "3/3
I6.PJ4
1
ia,
1 2
-21.S 7
I 7^^>
? /,
1 //^

1
5?,5-r
1 /
/
1 79^

I
Q
T


-3&

%



"75''.

"^7;

[^!

lD\

1

	I
1
i
1
~i
1

1
l
\
I

1	
i
1
/
FORM I SV-TIC
1/87 Rev.

-------
13
SEMIV0LATIL2 ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: Leak, hgird Contract:£/$tT?-3|	^ ^
Lab Code: 	 case No. v^^S^hvVsAS No.: 	 SDC No.:
Matrix: (soil/water) 10! U
Sample vt/vol:	"3£>6 (q/aL) C~
Level: (lov/med) L.C Lv
\ Moisture: not dec. O , I dec.	
Extraction: (SepF/Cont/Scnc) 'SC-aJC^
GPC Cleanup: (Y/N) V	pH:
CAS NO.
COMPOUND
Lab Sample ID: ^	^
Lab File ID: 7*^5^ S
Date Received: ~*7/s--5
Date Extracted: ~7f2-7
Date Analyzed:
Dilution Factor: /, C'
CONCENTRATION UNITS:
(ug/L or ug/Xg) U /j* I	Q
108-95-2-
111-44-4	
95-57-3	
541-73-1—
106-46-7—
100-51-6—
95-50-1	
95-48-7	
108-60-1—
106-44-5 —
621-64-7 —
67-72-1	
98-95-3	
78-S9-1	
88-75-5 —
105-67-9-
65-8S-0—
111-91-1-
120-83-2-
120-82-1-
91-20-3 —
106-47-8
87-68-3-
59-50-7-
91-i 7-6-
77-47-4-
S8-06-2-
95-95-4-
91-58-7-
58-74-4-
121-11-3
208-96-8
606-20-2
	Phenol
-b is (2-Chloroech.y 1) ether^
- 2 -Ciil o r opheno 1_

¦I,3-Dichlorobenzene_
•1,4-Dichlorobenzene"
»3enzyl alcohol^
¦1,2-Dichlorobenzene
-2-Methylphenol
bis(2-Chloroisopropyl)ether_|
—4 -Methylpheno 1	i
—N-Nitroso-di-n-propvlamine	|
—Hexachlorcethane	I
—Nitrobenzene	I
—Isophorone
	2-Nitrophenol.
—2 , 4-Dimethylphenol_
—Benzoic acid
1 ~2.£>&
-bis (2 -Chloroethoxy) methane	|
—2 , 4-Dichlorophenol	|
—1,2,4-Trichlorobenzene	I
—Naphthalene
UP
—		4 -Chloroaniline	
———Hexachlorobutadiene
—4-Chloro-3-methylpheno1_
—2-Methylnaphthalene_
—Hexachlorocyclopentadiene	__|
—2, ; , 6-Trichlorcphenol	_J
—I, •;, 5-Trichlorophenol	I
—2-Chloronaohthalene	I
--2-Ninroaniline			'
—Dime thy lphthalate_	I
—Acenaphthylene


_22=0*.

	2', 6-Dinitrocoluene

I !
FORM I SV-1
1/87 ¦

-------
1C
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name
Lab Code:
; Laa k ItesJ ^ <£¦	Contract: A&-05 ~ J 2/Z$
______ Case Ho. -.4/IoJm. U*J SAS No.: 	 SDG No.:

Matrix: (soil/water) ^£7_Z_
Sample wt/vol:	(g/mL)
Level: (low/med) £-£ k/
% Moisture: not dec. <3 , / dec.	
Extraction: (SepF/Cont/Sonc)
GrC Cleanup: CY/N)	pH:	
Lab Sample ID: *7^ /& *7
Lab File ID: ?
CAS NO.
COMPOUND
Date. Received: ~7 f
Date Extracted: 7/27/5^
Date Analyzed: *9 /2-/> °!
• Dilution Factor: / ¦ O
CONCENTRATION UNITS.:
(ug/L or uq/Kg) UL-)U.C~ Q
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-6	
101-55-	3	
118-74-1	
S7-86-5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-8	
193-39-5	
53-70-3	
191-24-2	
- 3-N itroan i1ine
-Acenaphtiiene
2,4-Dinitrophenol_
¦4 -Nitroptienol	]
Dibenzofuran
¦2,4-Dinitrotoluene
¦Diethylptitiialate_
4-chlorophenyl-pheny lecher
——Fluorene		
•4-N itroaniline	
-4,S-Dinitro-2-mecaylphenol	
-N-Nitrosodiphenylamine (1)
-4-3rcmophenyl-phenylether	
-Hexaciilorobenzene	
-Pentachlorophenol	
-Phenanthrene	
-Anthracene
—Di-n-butylphtftalate_
—Fluorantbene	~
—Pyrene_
—Butylbenzylphtftalate	
—3 ,3 ' -D. -.lorobenz idine
—9enzo(a nthracene	
—Chrysene
-bis(2-Ethyihexyl)pntnalat.e.
—Di-n-octylpnthalace	 ¦
—3enzo(b)fluoranchene	
--Senzo(k) fluoranchene	
—3enzo(a)pvrene
-Indeno(1,2,3-cd)pyrene
-Oibenz(a,h)anchracene_
-3enzo(g,h,i)perylene	


3 "2eo

1-i.C; C>

k6C



UJL

660
A*-
2CC
7 2. 6

JL


±
LL
1)
- Cannot be separated iron Oipnenylamme
FORM I SV-2
1/87 Rev.

-------
IF	SPA samfl:
SEMIVOLATILE CRGANICS ANALYSIS DATA SHEET-
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Naae; L-gc h frfJ~~ fz $£. Contract: 6^~«J3-"?zy7 j /"/ & J
Lab Cede: 	 Case Ho.: McfalinJsxs Mo.: _____ SDG Mo.:
Matrix: (soil/water) *5Q tL«	Lab Sample ZD: C! 3 }&
Sample wt/vol:	?£ (g/aL) &*	Ub File ID:	3|
Level: (lov/aed)	Date Received: 7/2 b /S
% Moisture: not dec. ^ » / dec.		Data Extracted: ~7/Z7y/*
4.

Aj rt Aft2 *1/ A/
1
y "*< £
5.

U- *J * „i/ a/
i-
2£>
6.

S*» Ae'£t: A/VJ ! c— / c/
12*.2>S I
2. *S" C-1
7 .,
*><» *V, ~
1 — ~ 1* f a/jS - > "? / - ^2, £ '/ive-fd**
1 27, !
?"*<£'!?
a.

1
1 1

0 _

1 d*Ji 
*>.
1 1
lr
13.

1 ^ ft A/J IV/V /-/vtJrt *£-*¦* iso ¦*/
1 J//Y7 i
/ /•
1 14.

1 L/a/XlyV/t/ /V vceV c ^ >£?«; "~
1 3/,7^3 1

[ 15.

I U Aj ft *S> u/f
1.3 I
1 7a 0
! 16.

\ (J vr-* *<} tf .4 j 4C.J&I* lao 
UfT.5"/ 1

I 19-

1 />' «s X ba rf a/
1 ¦}<"!,Z"7 |

I 20.

I
1 1

1 21.

I
1 ' 1

I 22.

1
1 i

[ 23.


! I

! 24.

1
! I

! 25.

s
! i

i 26.

1
: 1

; 27.

!
1 i

I 23.

I
1 1

1 29.

1
1 1

! 30.

1
( 1


FORK I SV-TIC
!/«¦

-------
13
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: L^^Contract\	^ ^^ ^
Lab Code: 	 Case No.	SAS No.: 	
Matrix: (soil/water) 'S&lU
Sample vrt/vol:	1C,C> (g/mL) G~
Level: (lov/med)
% Moisture: not dec, d < O dec.	
Extraction: (SepF/Cont/Sonc) 'yQ/JC-
G?C Cleanup: (Y/N)_Y_	pH:	
	 SDG No.: 	
Lab Sample ID: ?5/
Lab File ID: ^U
Date Received:
Data Extracted: *7 J 1^/S*7
Date Analyzed:
Dilution Factor:
} ,6
CAS NO.
COMPOUND
CONCENTRATION UNITS:..
(uq/L or uq/Xq) }J/*- /K£~ Q
108-95-2-
111-44-4—
95-57-8	
541-73-1-
106-46-7-
100-51-6-
95-50-1—
95-48-7—
108-60-1-
106-44-5-
621-64-7-
67-72-1——
98-95-3—
78-59-1 —
88-75-5—
105-67-9-
65-85-0—
111-91-1-
120-83-2-
120-82-1-
91-20-3—
106-47-8
87-68-3-
59-50-7-
91-i 7-6-
77-47—4—
38-06-2-
95-95-4-
91-58-7-
S8-74-4-
131-11-3
208-96-8
606-20-2
	Phenol
¦bis (2-Chloroethy1) ether_
-2-Chlorophenol_
¦l,3-Dichlorobenzene_
¦1,4-Dichlorobenzene~
•Benzyl alcohol.
•1,2-Dichlorobenzene_
•2-Methylphenol_
¦bis(2-Chloroisopropyl)ether
•4-Methylphenol
—H-Nitroso-di-n-propylamine	
—Hexachlorcethane	
—M itrobenz ene	
—Isophorone
	2-Hitrophenol_
—2,4-Dimethylphenol_
—Benzoic acid 	
—bis(2-Chloroethoxy)methane	
—2,4-Oichlorophenol
—1,2,4-Trichlorobenzene_
—Naphthalene,
	-4-chloroaniline
	-Hexachlorobutadiene
—4-Chloro-3-methylphenoi.
—2-Methylnaphthalene,
—Hexachlorocyclopentadiene	
—2,4,6-Trichlorophenol	
—2,4.5-Trichlorophenol	
—2-Chloronaohthalene	
—2-Nitroaniline	
—Qimethylphthalate_
—AcenaphthvLene_
	2,6-Oinicrotoluene_
±LO\_0.
- /
3 tO\

t 2-C O
&£ d)
JL2^2:
<•*
£
I

FORM I SV-L
1/8 7 P.ev.

-------
1C
EPA SAMPLE a4U
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
Lab Name: L-yc.U h	Contract:	
Lab Code: 	 Case No.:	S AS No.: 	
X '*2-2 $
I
SDG NO.
Matrix: (soil/vater) "5CIL.
Sample vt/vol:	?C , 0 (g/mL^ 0"
Level: (lov/ned) u£ Li/
% Moisture: not dec. 0 dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: CY/N)_X-		
CAS NO.
COMPOUND
Lab Sample ID: ^ [6&
Lab file ID:
Date Received: T
Date Extracted: 2l2£l5J
Dac* Analyzed: ^
Dilution Factsr: / > &
CONCENTRATION UNITS:
(ug/L or ug/Kg) U6-Jkc- Q
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-6	
101-55-	3	
118-74-1	
S7-86-5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-0	—	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-3	
193-39-5	
53-70-3	
191-24-2	
-3-Nitrcaniline_
-AcenaDhtiiene
•2,4-0initrophanol_
-4-Nitroph.anol
-Dibenzofuran
•2,4-Dinitrotoluene_
-Dietiiylphthalate_
-4-Chloropnenyl-piienylet.t:er	
¦Fluorene 	
	-4-Nitroamline
•4, S-Dinitrc-2-metbylpnenol	
-N-Nitrosodiphenylamine (1)	
-4-Brcmophenyl-phenyletter	
-Kexactilorobenzene	
-Pentachlorcphenal	
-P^enanthrene	
-Anthracene
¦Di-n-butylphthalate_
—rluorantbene
—?yrene_
—Sutylbenzylphtftalate	
—3,3'-0. -.lorobenzidine
—3enzo(a nthracene	
-CJirysene
-bis(2-Etiiyl.nexyl) pntnalate	
-Di-n-octylphtbalace		
-Senzo(b)fiucrantnene
--=enzo(X)fluorantnene	
—2enzo(a)pyrene	
— Indeno (1,2,3-cd) pyrene,
—Oibenz(a,h)anthracene_
—3enzo(g, h,i)perylene	
3 2.(2 C
U
bh O
A •? /? (sC I
±Z<'
; zgc !
U>o
J*.

&

7W

V
?6C' I ~jR
A ! U
(1) - Cannot be separated :'rom Dipnenylamine
rnflM r
l /«•

-------
Lab Name:
Lab Code:
Matrix: i
soil/water)*^OIL~
Extraction;
G?C Cieanuo:
IF	EPA SAMPLE NO.
SEMIVOLATILZ ORGANXCS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS	|
Lttkh tzg'J	Contract: 19 ~^S"3 \ ^
	 Case Mo. :/EMWWsaS No.: 	 SDC No.: 	
Lab Sample ID: ^ £d
Lab File ID: 'P
Date Received: ^Z.
/* Gh f
Date Extracted: 7 /'*¦ 5-/35
Date Analyzed:
Dilution Factor: / , &
Sample vt/vol: "5 O (q/mL) f r-
Level: (low/med) L£wJ
\ Moisture: not dec. 0 > & dec.	
(SepF/Cont/Sonc)
(Y/N) V
?Q/j£
oH:
Number TICs found:
CONCENTRATION UNITS: >uy
(uq/L or uq/Xq) V fr- t KO~
CAS
NUHBER
| COMPOUND HAKE
RT |
EST. CONC.
Q 1
1.
	
1 r'JAJA*/ aJ

/7a*
¦T j
2.
	
\.j H/ V A/vj fiPcoA £Pe- -/
"7 O & 1

! 'Ml
3.

VJ-J X *#**«/ hi**//***# Ifi,* iS
-T-i* 1
 jn/ MvsS K? &S "V
i#.4* i
/ \/9
1 • fO:
a ,
	
1 tj -V M I* €* >^S IS
1 1.H-1 1
? 7fJ
! ' p\
10.
..
1 // 1/ fit Hti u> -l/


1 i !
11.
—
1 1/hi -m* -V
1 A*,Z7 '
/ L$D
1 : i
12.

1 ! /+/hC tst s> \.%S "%/
1 /&, ? <3
H S*,
I i i
13.
	 			
1 IS'** ft *a */ */
1 /g.*ir3
1 O DC
1 \i——t
14.

1

1 I
IS. 1 till
16. I III!
17. 1 II II
18. 1 II 1 !
19. 1 II 1 I
20. 1 1 r I 1 :
21.

1
1

1 !
22.

1
1

1 !
23. 1 1 1 i
24. [ II!-
25.


1
1
1
26.

1
1
1
f
27.

1
1
1

28.

1
1
1
1
29.

1
1
1
1 !
20.

i
1
1
! !
FORM I SV-TIC
1/8? Rev.

-------
ib
SEMIVOLATILZ ORGAN ICS AilAL^SIS DATA SHEET
Lab Name: / gc kk	$<£¦
Lab Code: 	
Contract: c^-^7-72 y*7
EPA SAMPLE"-
d ~2- !
	Case No.: /^ij^/wSAS No.:
Matrix: (soil/water) *50!£~~
Sample vt/vol:	10.-& (q/nL)
Lavel: (lov/med) LC Vu
\ Moisture: not dec. ^	dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N)jV	pH:
SDG No.:
Lab Sample ID: *7 5' / ^
Lab File ID:
Date Received:
Date Extracted:
Date Anal/zed: ?///£?
Dilution Factor:
A <2
CAS NO.
COMPOUND
CONCENTRATION UNITS: ,
(ug/L or uq/Kg)cJ/j-7
108-95-2	
—Phenol
111-44-4	
—bis(2-Chloroethvl)ether
95-57-8	
—2-Chlorophenol
541-73-1	
—1.3-Dichlorobenzene
106-46-7	
—1.4-Oichlorobenzene
100-51-6	
—Benzvl alcohol
95-50-1	
—1.2-Dichlorobenzene
95-48-7	
—2-Methvlohenol
103-60-1	
—bis (2-Chlorqisopro'pyl) ether_
106-44-5	
—4-Methy1pheno1
621-64-7	
—N-Nitroso-di-n-propylarame
$7—72 — 1———
—Hexachloroethane
98—95—3	
—Nitrobenzene
78-S 9-1	
—Isophorone
88-75-5-——-
—2-Nitrophenoi
105-67-9	
—2.4-DimethylDhenoi
a*
in
1
CD
in
1
0
1
1
1
1
1
1
1
—9enzoic acid
111-91-1	
—bis(2-Chloroethoxy)methane__
120-83-2	
—2.4-Dichlorochenol
120-82-1	
—l.2 f4-Trichlorobenzene
91-20-3	
—Naohthalene
106-47-8	
—4-Chloroaniline
87-68-3	
—Hexachlorobutadiene
59-50-7	
-—4-Chloro-3-methvlohenol
91-i 7-6	
	2-MethylnaDhthalene
77-47-4	
	Kexachlorocyclopentadiene	
38-06-2	
	2. 4 . 6-Triciilorochenol
95-95-4	
	2 . 4 . 5-Triciiloroohenol
91-58-7	
---2-Chlaronaotithalene
38-74-4	
—-2-N itroaniline
131-11-3	
-—Qimethylphchalate
208-96-3	
-—AcenanhthvLene
606-20-2	
	2.6-Oinitrotoluene
to4r &

1-2.0 O
hJ2
3 -1.&C
tub O
-/ "2.0 0
(2 6 c-
a















IX
FORM I SV-1
i/a7"

-------
1C
EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET		
I
: Laa.^- h Contract: ^-£>^-32^^ | ^ ^
	case Mo. ^e-^/^v/sAS No.: 	 SOG Ho.: 	
Lab Name
Lab Code:
Matrix: (soil/water) fyC}i-
Sample vt/vol:	?&,& (g/mL) 6-
Level: (low/ned) LC \aJ
% Moisture: not dec. OxO dec.
Lab Sample ID: ^J~70
Lab File ID: >Z.'7<£7' *7
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: CY/H) V	pH:	
Date. Received:
Date Extracted: ~7 f^y I*?*?
Date Analyzed:
Dilution Factor: /. C
CAS NO.
COMPOUND
CONCENTRATION UNITS:.
(ug/L or ucr/Kq) lJc~/{6£-
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-6	
101-55-	3	
118-74-1	
37-86-5	
35-01-8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-8	
193-39-5	
53-70-3	
191-24-2	
-3-Nitroaniline_
-Acenaphttiene_
¦2,4-Dinitrophenol_
-4-Nitrophenol	~
-Dibenzofuran
-2,4-Dinitrotoluene
•Diethylphttialate
4 -Cl\lo rophenyl-phenyls tiier	
Fluorene 		
-4-Nitroaniline	
-4,6-Dinitro-2-aetiiylphenoi	
-H-Nitrosodiphenylaoine (1)	
-4-Brcnophenyl-phenylether	
-Hexachlorobenzene	
-Pentaciilorophenol	
- Phenanthrene	
-Anthracene
—Di-n-butylphtHalate
—Fluorantiiene	
--Pyrene
-Butylbenzylphtiialate	
-3,3'-D. ilorobenzidine
-Benzo(a nthracene	
drysene
—bis (2-Ethylhexy 1) phtfcalate	
—Di-n-octylphthalate		
—3enzo(b)fluoranthene	
—Senzo(k) fluorantiiene	
—3enzo(a)pyrene
-Indeno(1,2,3-cd)pyrene_
-Oibenz(a,h)anthracene^
—3ehzo(g,h,i)perylene	
\<2  VFL .of*#
-U~-
(1) - Cannot be separated :roa Dipnenylaoine

-------
SEHIVOLATILE ORGANXCS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE K
Lab Naae
Lab Code:
: L>/!*k hEF?J - E*?£- Contract: | ^ )
	 Case No.	SAS No.: 	 SDG No.: 	
T
Matrix: (soil/water) ^OiL
Sample vt/vol:	(q/aL) fr-
Level: (low/aed) L£ lu
% Moisture: not dec. & & dec.	
Extraction: (SepF/Cont/Sonci
GrC Cleanup: (Y/N) V	pH:	
Lab Sample ID: 5 / *7<^
Lab File ID: 7^ 5dl 7 "1
Date Received:
Date Extracted: ~7 /2.~7 /^M
Date Analyzed:
Dilution Factor:
/
/O
Number TICs found:
CONCENTRATION UNITS:
(ug/L or uq/Xg) U A>tU6-
CAS NUMBER
1.
COMPOUND KAME
EST. COHC.
vnMatatatssi
' zee#
2.
! CJ
1 6 ,*7 / I
1 HGfi
3.7** ^ V 4>
1 BSha-e >,/.>.J. !/> rlsl
I 1
?
4.
I <£
8. 1 1
9,
I t J M nt? v*S «- Ajk?'*V
U«.?«7 1
i*Cf ft
10.
1 Xn) 1
z~:oO
12.
1
J-

13.



14.
1 (J A/ tt AS S\S
1 3^.2/ 1
^ >a
IS.
1 U *v >,L'VW hi-.to #aa*Al3et*s
I ¦? I
<***£)
16.
1 (Ss '
1 "? /, 1
t*T6G
17.
1 U*sK h4s,ct
1 3 ?,*?¥ 1
t 2 <3A
13.
| £/-v Afi,i'viV si 2 £ * *> be* IS"
1 fJ.^1 1

19.
I
\?<:W 1
¥3£>C>
20.
1
i - 1

I	21..
I	4. 2.
I	23."
I	24 .
:	25."
I	26.
;	27."
I	2a.'
1	29."
!	20.*
FORM I SV-TIC
1/8".

-------
IB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: Lae.k h&sa-fc	 Contract:AG-d3~32if |
Lab Code: 	 Case No.	SAS No.: 	 SDG No.

Matrix: (soil/vater)
Sample vt/vol:	(q/mL)
Lavel: (lov/med) 1~C>\a/
* Moisture: not dec. 0, 2- dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N) ^	PH:	
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted: "7 f'Z 7 fa f
Date Analyzed:
Oilution Factor:
aA
CAS NO.
COMPOUND
CONCENTRATION UNITS;
(ug/L or uq/Kq) t;A-/^6*
I
108-95-2	
111-44-4	
95-57-8	
541-73-1	
106-46-7	
100-51-6	
95-50-1	
95-48-7	
108-60-1	
106-44-5	
621-64-7	
67-72-1	
98-95-3	
78—b9—1	
88-75-5	
105-67-	9	
65-85-0	
111-91-1	
120-83-2	
120-82-1	
91-20-3	
106-47-	8	
87-68-	3	
59-50-7	
91-i 7-6	
77-47-4——
88-06-	2	
95-95-4	
91-58-7	
38-74-4	
131-11-3	
208-96-8	
606-20-2	
——Phenol
',10
¦bis(2-Cftloroethy1)ettter_
- 2 -Chi o r opheno 1_
¦1,3-Dichlorobenzene_
¦1,4-Oichlorobenzene"
¦Benzyl alcohol.
•1,2-0ic&lorobenzene
¦2-Methylphenol
bis(2-Chloroisopropyl) ether_|
—4-Methylphenol	1
—N-Hitroso-di-n-propyiamine	j
—Hexachloroethane	|
—N itrobenz ene	I
—Isophorone,
—-2-Kitrophenol_
—2,4-Dimetiiylphenol.
—Benzoic acid
—bis(2-Chloroethoxyjmethane	|
—2,4-Oichlorophenol	I
—1,2,4-Trichlorobenzene	|
—naphthalene

f\l O
1
—4 -Chloroanil ine	
	-Hexachlorobutadiene
—4-Chloro-3-aethylphenoi
—2-Methylnaphthalene
-Hexachlorocyclopentadiene__|
—2.4, 6-Trichiorophenol	I
—2,4, 5-Tricftlorophenol	I
—2-Chloronaphthaiene	 I
-2-Nitroaniline	
—Oinethylphthalate_
—Acenaphthy Lene

6 7 O
T2d?<2
I
6YO
	2,6-Oinitrotoluene_

o



-------
1C
S"FMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE S.
Lab Name: kh/*&J	Contract: <£3^ 1 ^
	 Case Ho. '.AlcBfi.Uha^9iS
Lab Code: 	
Matrix: (soil/water)
Sample wt/vol: 1&./0 (g/mL) 6"
Level: (low/med) £-£ \as
% Moisture: not dec. O > 2- dec.	
No.
SDG No.
Lab Sample ID:
Lab File 12:
o

1
Extraction: (SepF/Cont/Sonc)
pH:	
Date. Received: 7/zzr/5?
Date Extracted:
Date Analyzed:
GPC Cleanup: (Y/N)_V
CAS NO.
Dilution Factor: /. &
COMPOUND
CONCENTRATION UNITS:y
(ug/L or uq/Kq) i>/-/ /Y^~
99-09-2	-	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3—
86-73-7	
1Q0-O1-6	
534-52-1	
86-30-	6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-8	
193-39-5	
53-70-3	
191-24-2	
—— 3-Nitroaniline_
	Acenanhtftene
	2,4-Oinitrophenol_
	4-Nitrophenol	~
	Dibenzafuran	
	2,4-Dinitrotoluene_
	Diethylphthalate_
¦—4 -Chlorophenyl-phenyletiier	
	-Fluorene
——4-witroaniline	
	4,6-Dinitro-2-metiiylphenoi	
	-N-Nitrosodiphenylamine (1)	
	4-3rcmophenyl-phenyletiier	
———Hexachloroben2ene
——Pentachlorophenol	
—	Pfrenanthrene
	-Anthracene	
	Di-n-butylphthalate_
—— Fluor anthene	~
——Pyrene
	Butylbenzylphthalate	
	3 ,3 ' -D. -,.lorobenzidine_
	9enzo(a nthracene	"
——Chrysene
	bis(2-Etiiylhexyl) pntnalate	
——Di-n-octylphthalate	
——3enzo(b)fluoranthene	
	5enzo()c) fluorancftene
—-—3enzo(a)pyrene	
	Indeno(1,2,3-cd)pyrene_
	Oibenz(a, h)anthracene^
	3enzo(g,h, i) perylene	
? 2-C?
6T/J
1 2.2 e

&j_o

] 2.0 L-
3Z


_=L.
i
ipia
¦b

lo
_=ki.
S-L


(1) - Cannot te separated :rom Oipnenyiamine
<>' !
I I
i I
XE'

FORM I SV-2
1/87

-------
If
SEMXVOIATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
SDC No.
Lab Name:	hjr£^	CantrdLCZ:6'£-a'?-3<2fc? j	/ / /
Lab Code: ________ Case No.: AUkJ>AS No.
Matrix: (soil/vaterS *701L
Sample vt/vol:	3 0 (g/nL)
Level: (lov/ued) L(j U/
% Moisture: not dec. O t ~~2— dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N) V	pH:	
Lab Sample ID:	! 6*1
Lab File ID: *7 <£L ~J £
Date Received: "7
Date Extracted:, ihf/SJ
Date Analyzed:
Dilution Factor: ) , &
Number TICs found:
CONCENTRATION UNITS:
(ug/L or ug/Xq) iJ6~l&C
CAS NUMBER
COMPOUND NAME
EST. CONC
1.
2."
3."
4 ."
5."
6.'
7."
10.
11."
12."
13."
14."
15."
16."
17."
18."
It."
20."
21."
22."
22."
24.'
25.'
26."
27."
28.'
29.'
20.'
U *S\tA/ti 14* ~t/
(y> A/	* tA/Sl/ '
¦MlHlHIIIIBlMMMHHnMWMMMBHHMNMMHn
U A/ ii4/a w A/
I t 3
*'2-* 1 7 hGfl

Js2£_
m\a |
M

-------
13
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE M(
/ 		\	7
Lab Name: L/o /L.
Sample vrt/vol:	3£>£ (g/mL) 6r
Level: (low/med) Z-^u/
% Moisture: not dec. &, C> dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N)


Lab Sample ID: J>)/!?/<4~2.
Lab File ID:
Date Received:
Date Extracted: 7/2^"/S*7 ®
Date Analyzed:
Dilution Factsr:
/, £
CAS NO.
COMPOUND
CONCENTRATION UNITS:,
(ug/L or ug/Xg) 0 6-iKO~
108-95-2	
111-44-4	
95-57-8	
541-73-1	
106-46-7	
100-51-6—	
95-50-1	
95-48-7	
108-60-1	
106-44-5	
621-64-7	
67-72-1	
98-95-2	
73-1:9-1	
88-75-5	
105-67-	9	
65-85-0	
111-91-1	
120-83-2	
120-82-1		
91-20-3	
106-47-	8	
87-68-3	
59-50-7	
91-i 7-6	
77-47-4		
38-06-2	
95-95-4	
91-58-7	
3 8-74-4	
131-11-3	
208-96-3	
606-20-2	
-Phenol	
-bis (2-caiaroet.kiyl) ether_
-2-Chlorophenol_
¦1,3-0ichlorobenzene_
-1,4-Dicftlarobenzene"
'Benzyl alcohol^
¦1,2-Dichlorobenzene_
-2-Methy1pheno1	
——4-Methylphenol_
—riexachloroethane_
—Nitrobenzene	
—Isophorone
	2-Nitroohenol
—2,4-Dimechylphenol_
—Benzoic acid	.
-—2,4-0ichlorophenol.
—1,2,4-Trichlorobenzen«_
—Naphthalene_
	4-chloroaniline	
——Hexachlorobutadiene
—4-Chloro-3-methylphenol_
—2-Methylnapnchaiene	
— 2,4, 6-Trichlorophenol_
—2 , 4 , 5-Trichlorophenol_
—2-Chloronaphtftalene
—2-Nicroaniline
—Dimethylphchalace_
—AcenaDhchyiene	
	2,6-Oinicrocoluene^
1
|











1 ' 1
1 1
! 1











1

I 3 -2.e?&
1















1

1 ? 1.0 o
1
1
1


1L
T
TZ.
FORM I SV-1
1/37 ?.

-------
1C
5EMIV0LATILE ORG AN ICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name
Lab Code
: Contract:(&-C"b~3¦2^*7'|	"7
	 Case Mo. i/^&y^/fri^SAS No.: 	
Matrix: (soil/water) _^V^_
Sample vt/vol: 1>Q,C (q/mL) /r-
Level: (lov/med) L/0 UJ
% Moisture: not dec. &	dec. 	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: CY/N) ^	pH:	
	 SOG Mo.: 	
Lab Sample ID: 5 / £~Z.
Lab File ID:
Date. Received:
Date Extracted: 7/2. £7^
Date Analyzed:
Dilution Factor: f .0
CAS NO.
COMPOUND
CONCENTRATION UNITS,
(ug/L or ug/Kg) U6- / fcc-j
V
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-	7	
100-01-	6	
534-52-1	
36-30-6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
213-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-3	
193-39-5	
53-70-3	
191-24-2	
-3-Nitroaniline
-Acenaphthene
-2,4-Dinitrophenoi_
—4-Witroohenol
—Dibenzofuran
-2,4-Oinitrotoluene
—Diethylphthalate
-4-Chlorophenyl-phenylether	
-Fluorene
—4 -Hitroaniline	
—4,6-Dinitro-2-nechylphenol	
—N-Nitrosodiphenylamine (1)	
—4-Bromophenyl-phenylether	
—Hexachlorobenzene	
—Pentachlo rcpheno1	
—Phenanthrene	
—Anthracene
—Di-n-butylphthalate
¦—Fluoranthene	
—Pyrene
—Butvlbenzylphthalate
—3,3'-D. -.lorobenzidine
~Benzo(a nthracene	
¦Chrysene
—bis (2-Ethy Lhexy 1) pnthalate_
—Oi-n-octylphthalate	~
— 3enzo(b) fluoranthene	
¦—3enzo(lc) fluoranthene	
¦—3enzo(a)pyrene
—Indeno(1,2.3-cd)pyrene,
—Oibenz(a, h)anthracene^
—3enzo(g,h,i)perylene	
33- O*

3 2.CC
6 £ &

-y

v
3
h6Q
JL
_3J2£.

1<7&
Ah£.

jJZ*L

1) - Cannot be separated from Oipnenylamme
V
1L

u
z:
FORM I SV-2
1/87 Rev.

-------
Lab Hase:
Lab Code:
IF
¦SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Look b BP J	Contract:		
	 Case No.: 	 SAS No.: _____ SDG No,:
SPA SAMPLf
L A &
Matrix: (soil/water} j^OjA
Sanole wt/vol:	1 ^ (g/aL)
Level: (low/aed) LP vJ
\ Moisture: not dec. & tCJ dec.	
Extraction: (SepF/Cont/Sor.cj
V
GrC Cieanuo:
(Y/N)
oH:
Lab Saaple ID: ^ 5/<£ 2L
Lab File ID:
Date Received: ~~7 (it £fyj
Date Extracted: 7 Ji eft I
Date Analyzed:
Dilution Factor: / > O ¦
Nuaber TICs found:
CONCENTRATION UNITS:
(ug/L or uq/Ko) l) c-/K&-
I CAS NUMBER
1.
2."
3."
4 .~
5."
6.:
7.
8-1
a
10 •
11."
12."
13."
14."
15.'
16."
17."
18.*
19."
20."
21.;
a 2.
23
24	.
25.'
26.
27.
2a.
29.
30.
ThT
COMPOUND NAME
J
RT
i» • "TV
:st. CONC.
	1 C.,
U	sv -d.ee a ft	J 7
7^
~ *<20

•J V < hct **»/ ¦ 1 Ram an<£
*1C
/ &£¦ C
\,J		1 7,2^ | H 2.0 C
I tJ v & U el s/a/ r-f-tS/i lilltI "7 *> )
1 Z-f-h*A/'S. / J. 1. > - T>= +£AfAJeSSA ** >j*
¦ I ^ ^ ^, 2 ^
I fy -*/ ^	kh7	lJan/7s. I *7. /
' '		liLE^LL
v«3£
I
i
FORM I SV-TTC
i/a<

-------
la
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
.	|	t	?
Lab Name: Lot, U.li)=	£	Contract: (j%-21-32-YI ^
T.ata code:
Case No. yrfez^tiiUreiSAS Ho.:
SDC No.
Matrix: (soil/water) b>C / L~
Sample vt/vol:	1C,Q (q/mL) (r
Level: (lov/aed) L£ it/
\ Moisture: not dec. > V dec.	
Extraction: (SepF/Cont/Sonc) A/c.
G?C Cleanup: (Y/N) V	pH:	
CAS NO.
COMPOUND
Lab Sample ID: ^ / 7 J
Lab File ID:
Data Received: 7
Date Extracted:
Date Analyzed: f ///
-------
1C
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE Su.
Lab Wane; /_g
Lab Code:
<.U	Contract: /£\ L* ^
Case Wo. :A?e,/%/*.U^JsAS No.
SOG No.:
Matrix: (soil/water)*pC>/L.
Sample vt/vol:	10,0 (q/mL) O-
Level: (low/ned) L£ hy
k Moisture: not dec; 2/ H dec.	
Extraction: (SepF/Cont/Sonc) 5CVC
G?C Cleanup: C*/N)Y_	pH:	
Lab Sample 10:
Lab File ID:
?5/7/
_2±2^11¥
Date Received:
Date Extracted:
Date Analyzed: ///&*^
Dilution Factor: / >0
CAS NO.
COMPOUND
CONCENTRATION UNITS:.
(ug/L or uq/Kg) Q/C/ kS-' Q
99-09-2	
—3-Nitroaniline
33-32-9	
—Acenaphthene
51-28-5	
—2.4-Dinitroohenol
100-02-7	
—4-Nitrophenol
132-64-9	
—Dibenzofuran
121-14-2	
—2.4-Oinitrotoluene
84-66-2	
—'Diethylphthalate
7005-72-3	
--4-Chloroohenyl-phenvlether
86-73-7	
—Fluorene
100-01-6	
—4-Hitroaniline
534-52-1	
--4,6-Dinitro-2-methylphenoi
86-30-6	
—N-Nitrosodiphenylamine (1)	
101-55-3	
—4-Broaophenyl-phenyletfter	
118-74-1	
--Hexacftlorobenzene
87-86-5	
—Pentachloroohenol
85-01-8	
—Phenanthrene
120-12-7	
—Anthracene
i
1
1
1
1
1
I
m
1
-3*3 I
±:\
1 ~*c &

i—'¦
I
t*ice i
ZZlZi
	=JtfS.1
l
-¦ i
3*

i' P 7

-------
IF
,semivolatile organics analysis data sheet
TENTATIVELY IDENTIFIED COMPOUNDS
>: Lac,kk EE.J p S
Lab Name:
T-»h Code: ______ Case No.:
Matrix: (soil/water) ^&]L:
Contract:
SAS No.:
EPA SAMPLE NO.
^ \ ~3
SDG No.:
Sample vt/vol:	1 O (q/mL) 0-
Level: (lov/med) j_£ i\/
% Moisture: not dec. 'Z ' *~l dec.
Extraction: (SepF/Cont/Sonc) £¦
G?C Cleanup: (Y/N)_V_	pH:	
Number TICs found: 	
Lab Sample ID: cf / "7 /
Lab File ID: y	7
Date Received:
Date Extracted:_ _7/Z7/f f
Date Analyzed: __
Dilution Factor:
///g 1
h o
CONCENTRATION UNITS:
(uis/L or ug/Kg) ujrjj^
CAS NUMBER
I COMPOUND NAME
1.

2. 7 7 W A
I £-}*a^s. /,/,£,2. --retri^c.^terta
3.
1 L/ iv *ts
4 .
1 U ^ s1/'d) iVxV

I £• '. *» sa is
6.
I u "J < 4/£ u/ /I/
7.

8.
1 L) */* A/+J H vs! Act./) !* k}0 is
9. 1
10.
1//'-/ U ma w /V•,& t?oe~4H b01/
11. iTTTflJ
! t* ,'rJ
12.
1 L/ Vm />A/ ,4iS
13.
| L/A/!£. ISI&VL/
14. 1
IS.
\U a; & svo *s * j
16. 1
17.
I O/v k -vj iv /V '
18.
1 L/ */ % ii & £'«• ~S
19.
I  >1/£. -4 fitoo-'IS
21. 1
22. 1
23. i
24. j
25.
26. !
27. f
28. |
29. |
20. i
RT
EST. CONC. | Q
£>*7 4a 1
2"J^
¦aa 1 aasoLi |
i T i
1
' "SJ
i
rj\
*,2.*r I
t/ £? 7A
i
• i
'fi.7 *i
'¦/>C
i

( 7,
? tc
i


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i

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Z3

i
i
2V.
?
i


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zt>.o 1
fen
i J


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i

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1 ! 1 <36
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Fc^miin r
WB7 ;ev

-------
15
SEMIVOLATILE ORGANIC! ANALYSIS DATA SHEET
EPA SAMPLE ! J
m	i		
Lab Name: Lt^^k A &IE6- ~~ *?<£¦	Contract
Lab Code: 	 Case Ho.: Ale. fA-d+hJ3 AS Ho.:
6*> -£>3 -72.99 ^ *7'^ ^
Matrix: (soil/water)
Sample vt/vol:	(q/mL) C~
Level: (lov/aed) L.C n/
\ Moisture: not dec. ?/*1 dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (VJH.il.		
	 SOC Ho.: 	
Lab Sample ID: c!*5 16 /
Lab File ID:

I
Date Received: "7
Date Extracted: "7 /2. 5 /*3
Date Analyzed:
Dilution Factor: ) > D
CAS HO.
COMPOUND
CONCENTRATION UNITS: .
(ug/L or ug/Xg) b>6- IM.&)
108-95-2—
111-44-4—
95-57-8	
541-73-1—
106-46-7—
100-51-6—
95-50-1	
95-48-7	
108-60-1—
106-44-5 —
621-64-7 —
67-72-1	
98-95-3 —
78-S9-1	
88-75-5—
105-67-9-
65-85-0—
111-91-1-
120-83-2-
120-82-1-
91-20-3 —
106-47-8-
87-68-3	—
59-50-7 —
91-i 7-6 —
77-47-4—
88-06-2	—
95-95-4 —
91-58-7 —
88-74-4 —
131-11-3-
208-96-8-
606-20-2-
Phenol	
bis(2-Chloroethyl)ether_
2-Chlorophenol_
•1,3-Dichlorobenzene
-1,4-Dichlorobenzene
-3enzyl alcohol	
¦1,2-Dichlorobenzene
•2-Methylphenol
bis(2-Chloroisopropyl)ether
4-Methylphenol
1 CAC\














1 1 1
--N-Nitroso-di-n-propylamine	
—Hexachloroethane
—Nitrobenzene	
—Isophorone
—		2-N itrooheno L
—2,4-Diaethylphenol_
—Benzoic acid
—bis(2-Chloroethoxy)methane^
—2,4-Dichlorophenol_
--1,2,4-Trichlorobenzene_
—Naphthalene^
—4-Chloroaniline	
—Hexachlorobutadiene
—4-Chloro-3-nethylphenol
--2-Methyinaphthalene
-Hexachlciracyclopentadiene	
-2,;,6-Trichiorophenol	
-2,4,5-Trichlorophenol	
-2-Chloronaphthalene	
-2-Nitroani.Line 		
—Oiraethylphtftalate	
—AcenachthvLene
— 2 , 6-Oinicrotoluene
I !
-XT
ncea


¦I
>2.
bG&!

ilEZi
7"
FORM I SV-1
V/8 7

-------
1C
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name
Lab Code:
; LaeJl k&eJ
Contract
:^£2l3^
Case
No.	No.:
SDG No.:
Matrix: (soil/water) ^(3/L-
Sample wt/vol:	1Q.O (g/mL)
Level: (lov/med)	It/
% Moisture: not dec.__3jJ~L. dec*	
Extraction: (SepF/Cont/Sonc) 5C_a/£-
G?C Cleanup: CY/N)j£_	pH:	
CAS NO.
COMPOUND
Lab Sample ID: ^ £ /
Lab File ID: 7~ t- <£¦ H K
Date. Received: 7 / *jg" h'y
Date Extracted: ~7 )'2-*rl<%e7
Date Analyzed: /2.*7
Dilution Factor: // £
CONCENTRATION UNITS:.
(ug/L or ug/Kg)Uj£j&) Q
99-09-2	
	3-Hitroaniline I

83-32-9	
——Acenaphtiiene I

51-28-5	
——2.4-Dinitrophenol I

100-02-7	
——4-Hitrophenol I

132-64-9	
	Oibenzofuran 1

121-14-2	
—¦— 2.4-Oinitrotoluene !


84-66-2	
	OiethvlDhthalate |


7005-72-3—
	4-Chlorophenyl-phanvletter |


86-73-7	
——-Fluorene 1

y
100-01-6	
——4-Nitroaniline 1

534-52-1	
	4,6-Dinitro-2-metHylphenol |

86-30-6	
——N-Nitrosodiphenylamine (1) I

101-55-3	
	4-BromoBhenyl-phenyletiier 1


118-74-1	
——Hexachlorctrenzene 1
>

87-86-5	
—— Pentactiloropftenol I
I?##
85-01-8	
	Phenanthrene 1
&<&c,
120-12-7	
——Anthracene 1
-vi__
84-74-2	
	Di-n-butvlphthalate I
A"
2-
206-44-0	
——Fluorantiiene 1
^<3
129-00-0	
	-Pvrene 1
!
85-68-7	
	3utvlbenzylphthalate 1

91-94-1	
	3.3' -D. -.lorobenzidine 1

56-55-3	
-----3enzo(a nthracene |

o
218-01-9	



117-81-7	
-----bis(2-Ethylhexyl) phtftalate. |
1 ? c
117-84-0	
	Di-n-octylphthalate 1

205-99-2	
———3enzo(b) fluorantiiene I


207-08-9	
	5enzo(k)fluoranthene !


50-32-3	
	Senzofa)pvrene I


193-39-5	
	Indeno(1.2.3-cd)pyrene 1


53-70-3	
	Oibenzfa.ft)anthracene 1


191-24-2	
	9enzofa.h.i)oerylene 1






(1) - Cannot be separated :roa OipnenyLaoine
=f=
X.
u

JA	!

FORM I SV-2
1/87 Rev.

-------
1«
..SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EfA SAMPLE H-.
Lab Haae
Lab Code:
: Lazuli erJ

Contract:^'3yi>' /^
Case Ho.: 	 SAS No.: 	 SOG No,
T
Matrix: (soil/water)
Saaple wt/vol:	6 (cr/mL) 6-
Level: (lov/aed) JLC ^
% Moisture: not: dec. J > H dec.	
Extraction: (SepF/Cont/Sonc; 'yCs/C*
G?C Cleanup: (Y/N) V	pH:
Lab Saaple IS:	U/
Lab File ID: 7L.V j
Date Received: 7/2£/S^
Date Extracted:
Date Analyzed: 0	^
Dilution Factor: f t ^
Kuaber TICs found:
CONCENTRATION UNITS i, . ./-
(ug/L or ug/ Kg) U Q- f K&—
*>?
CAS NUMBER
1.
2."
3."
4."
5
6."
7."
8."
g _ ~
10*
11.
12.'
13."
14.'
15/
16.
17."
18.
19.'
20.'
21/
23.'
24 .
25.
26."
27
28.'
29.
:o.
COMPOUND NAME
¦!	———
.1 ' ' A!
>J A/ y vS <*/
I UA/ri Hg	.V^' AQC A A
	i •>' "/*' iv'-v V/g-.- A {<=¦<+*> ksa is
H V \2L-t *7 •*/?*. t J, Z.
I 14 h •>
'is*
.1 /J h <9 Li/ 1/
_1 CS*//Sus
c-> V haV1/
I tx ./K*10-AS"	
RT
6	• 3 *>
—CLlSlS.
IS
7	¦ z.y
^
3j-ZL
HZS5
222!
/ f ^ —y
EST. CONC.
mans
_Z^_
/
/•T
I Z ^ 4?
.)__7.
A" ">
zj£.
122
-2LM
; «?^Z>
3 VP
73<£
1 /*. 24* 1 3
J/iLZ ~ " ~

MA
.\22dt£
XSO-
\4

--I-
FORM I SV-TIC
1/87

-------
IB
SZMIVOLATILZ QRGAKICS ANALYSIS DATA SHEET
Lab Name: L-Q L^C^T
Date Received: **7
Date Extracted: ~7 fD-
Date Analyzed: 9//hi
Dilution Factor: /. O
CONCENTRATION UNITS:
(ug/L or uq/Xq) 1)6-1X6- Q
108-95-2	
111-44-4	
95-57-3	
541-73-1	
106-46-7	
100-51-6	
95-50-1	
95-48-7	
108-60-1	
106-44-5	
621-64-7	
67-72-1	
93-95-3	
78-£9-l	
88-75-5	
105-67-	9	
65-85-0	
111-91-1	
120-03-2	
120-82-	1	
91-20-3	
106-47-	8	
87-68-	3		
59-50-7	
91-i 7-6	
77-47-4—	
88-06-	2	
95-95-4	
91-58-7	
38-74-4	
121-11-	3	
208-96-3	
606-20-2	
-—Phenol
•bis(2-Chloroethyl)ether,
• 2-Chioropheno1_
•1,3-Dichlorobenzene_
¦1,4-Dichlorobenzene~
•Benzyl alcohol_
•1,2-Dichlorobenzene_
¦2-Methylphenol_
¦bis(2-Chloroisopropyl)ether_
•4-Methylphenol
640
—N-N itroso-di-n-propylamine
—Hexachloroethane
—Nitrobenzene	
—Isophorone
—-2-N itropheno1_
—2,4-0imethylphenol_
—Benzoic acid '	"
—bis(2-Chloroethoxy)methane	
—2,4-Dichlorophenol
—1,2,4-Trichlorobenzene_
—Naphthalene
——4 -Chloroanilme	
——Hexachlorobutadiene
—4 -Chloro-3-methylphenol.
—2-Methylnaphthalene	
—2, 4 , 6-Trichlorophenol_
— 2, 4 , 5-Trichlorophenol_
—2-Chloronaphthalene	
—2-Nitroaniline	








1 		

[ "J H <3 ls \
1 M O 1

















1


-------
1C
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: Lac'k. fa	Contract :£&-£^~~32y^ |
Lab Code:	Case Wo.: Akfcfi/sfrd S AS No.: 	 SDG No.: 	
Matrix: (soil/water)
Sample vt/vol:	36,0 (g/mL)
Level: (low/med)	liJ
% Moisture: not dee. V, ^ dec.	
Extraction: (SepF/Cont/Sonc) 5*^^-
G?C Cleanup: CY/N)_^_	pH:	
Lab Sample ID:

Lab File ID: ^ ^-5^7#
Date. Received: JZh£ll?
Date Extracted:_ 7/z 7/5
Date Analyzed:
Dilution Factor:
UL
CAS NO.
COMPOUND
CONCENTRATION UNITS: .
(ug/L or ug/Kg) t} (r!<6~
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-	6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
213-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-3	
19 3-39-5	
53-70-3	
191-24-2	
-3-Nitroaniline_
-Acenaphttiene_
¦2,4-0initrophenol_
¦4 -Nitrophenol	~
-Oibenzofiuran
•2,4-Dinitrotoluene_
¦Dietiiylphthalate_
•4-Chlorophenyl-phenylether	
¦Fluorene		
	4-N itroani1ine
•4,6-Dinitro-2-methylphenoi	
•N-Nitrosodiphenylamine (1)	
•4-Bromophenyl-phenylether	
•Hexachlorobenzene	
•Pentachlorophenol	
-Phenanthrene
¦Anthracene	 ¦
~Di-n-butylphthalate_
—Fluorant&ene
—?yrene_
—Butvlbenzylphthalate
—3,3'-0- ilorobenzidine_
~3enzo(a nthracene	
-Chrysene_
—bis(2-Ethylhexyl)phthalate.
—Di-n-octylphthalate	
—Benzo(b)fluoranthene	
--=enzo(k)fluoranthene	
—Senzo(a)pyrene	
—Indeno(1,2,3-cd)pyrene	
—Dibenz(a,h)anthracene	
—3enzo(g,h,i)pervlene

12L






JLlZ.
±

a
J£&-
6 4 &

fie*

-------
IF
SEHIVOLATILE ORGANICS ANALYSIS DATA SHEET
TEHTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE MO.
I
Lab Nana: L~ G*- ^	^ t? contract: 6 £	i *2 f &
Lab Code: 	 Case Ho.:	Ho.: 	 SDG No.: 	
Matrix: (soil/water) 5&I
Sample vt/vol;	3 O (q/aL) 6~
Level: (low/aed) uO ^
% Moisture: not dec. Hdec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N) Y	pH:	
Lab Sample ID:
Lab File ID:	&
\W
Date Received:
Date Extracted: 1
Date Analyzed:
Dilution Factor: / r &
Number TICs found:
CONCENTRATION UNITS: . y
(uq/L or uq/Ka) (J6* / K6—
CAS NUMBER
COMPOUND NAME
I RT | EST. CONC.
I	I.,
I	2.
I	3.,
I	4.
|	S.
I	6.'
I	1-
I	8.
I	9-
I	10.
1	II.
I	12.
!	13.
I	14.
I	15.
I	16.
i	17.
1	18.
I	13.
1	20.
1	21.
I	22.
I	23.
1	24 .
I	23.
I	26.
i	27,
I	28,
I	2f,
i	20,

tj Vd'
1 ^,79. 1
tyoo
1 -5-, 1
£.^hAA/p. /, /, t. jr- f-etZA^hien*
1 1
*7*7 /9

U «/>^ AjbvitA/
1 0
1 1
(J A/ < /VV l/V /V
\ *.6 A 1
*6D
i I K\
V */ •£ AA3*a/A/
1 ^,"73 1

1 -rU'to
1 1 i :

1 9 1
/ 7(5/;

(/*/ vr* l¥^J#••*!**jas^S
1 1

I :
ll i i

-------
13
SEMIVOLATILE ORGAN ICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: Lod'U-loEbJ	Contract: 69	| " ^
Lab Code: 	 Case Ho.	SAS No.: 	 SDC No.: 	
Matrix: (soil/water) 'jOlL-
Sample wt/vol:	, £ (q/mL) C"
Level: (lov/med) LOW
\ Moisture: not dec. &/ *~f dec.	
Extraction: (SepF/Cont/Sonc) *5C
GPC Cleanup: (Y/N) V'	pH:	

Lab Sample ID: 	
Lab File ID:	V ^
Date Received: Tlz-rhf
Date Extracted: ~7)~2-b /S'7'
Date Analyzed: jS/i2l2!l
Dilution Factor: / • &
CAS NO.
COMPOUND
CONCENTRATION UNITS:.
(ug/L or ug/Kg) u£-/£0 1

1 S8-74-4	"J-Nitroaniline ! b fo C \

1 131-11-3	OimechylDhthalate . J
1

I 2Q8-96-3	kcenaphthvlene , 1
1

| 606-20-2—	2 . S-OinitrocoLuene m
l

1 1
		1 -

FORM I SV-1
1/37

-------
1C
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name
Lais Code:
: IlBsJ
Case Ho.
Contract:
AS No.

SDG Ho.
Matrix: (soil/water) *5£>/L.
Sample vt/vol:	ID. £> (g/mL) 6-
Level: (low/aed) /^£iaJ
% Moisture: not dec. (1, M dec.	
Extraction: (SepF/Cont/Sonc) ^ AJd.
G?C Cleanup: C*/N)j/	pH:	
Lab Sample ID:	)£ 7*
Lab File ID:	7
CAS NO.
COMPOUND
Date. Received: 7
Date Extracted: 7 ! 2.
Date Analyzed: ^ 12.^/^V
Dilution Factor: (r &
CONCENTRATION UNITS;
(ug/L or uq/Kg) L>fc* ( K6~ Q
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-	6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-31-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-3	
193-39-5	
53-70-3	
191-24-2	
-3-Nitroaniline
-Acenaphtiiene
2,4-Dinitrophenol_
•4-Nitrophenol	[
Dibenzofuran
-2,4-Dinitrotoluene_
-Diethylphthalate_
-4-Chlorophenyl-phenylether	
-Fluorene
—4-Nitroamline	
—4,6-Dinitro-2-methylphenol	
—M-Nitrosodiphenylamine (1)	
—4-Bromophenyl-phenylecher	
—Hexachlorobenzene	
—Pentachlorophenol	
—Phenanthrene	
—Anthracene
—Di-n-butylphthalate
—Fluoranthene	|
—Pyrene
-Butylbenzylphthalate		
—3,3' -D. -.lorobenz idine
—3enzo(a nthracene		
—Chrysene
—bis(2-Ethylhexyl)pnthalate	
—Qi-n-octylphthalate		
—3enzo(b)fluoranthene	
—3enzo(k)fluoranthene	
—3enzo(a)pyrene
-Indeno(1,2,3-ed)pyrene
-Oibenz(a,h)anthracene_
-3enzo(g,h,i)perylene	
3 "2.QC

3 Tt-C O
^ 2.0 0

^leL
-za &



3 i&c

JJL
±L&_


the
I loO
jxa
_LS£.
JJt£L
J=££.
ucc
h,6C

±Q.
(,o

U
1 !









!
1 ¦,!








X I
1 1
1 X 1
I T 1


¦JL
(1) - Cannot be separated froa Dipnenylanine
FORM I SV-2
1/87 Rev.

-------
IF
SEHXV0LATIL2 ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE Hi.

Lab Name: /.aa kh EpJ E^C-	Contract:
Lab Code: _____ Case No.: 	 SAS No.: 	 SDG No.
Matrix: (soil/water) ^0)L.
Sample vt/vol:	9 0 (c?/aL) £r
Level: (lov/med) LQ ti/
% Moisture: not dec. Q> Lf dec.
Extraction: (SepF/Cant/Sor.c) 5^^
GFC Cleanup: (Y/N)pH:	
Lab Sample ID: *?/4 *3
Lab File ID:	V
Date Received:
Date Extracted: *7
Date Analyzed:
Dilution Factor
/
O
Number TICs found;
CONCENTRATION UNITS r .
(ug/L or ug/Kq) Q6rf KC-
NAKE
COMPOUND
/ AJ K s*S<4 U/
1.
2.
3."
4 ¦
5."
6."
7."
8."
a _"
10."
11."
12."
13.'
14.'
15.'
16."
17.'
ia.
19.
20.
21.
a 2.
23.'
24 .
25.
26.
27.
28.
29.
20.
i/ SV K sv O isJ xt7
y -?
1 t; a/ M. AS O «/ Hvet A eeAiljOfAj \ ~7 , i h
7*0*^ Ifflw. J./ Z7.Z>

\ a

i *7 CO
I. /	it -I	Q.
3 ?. tr > I
)6-?c » tec#
7
I


FORM I SV-TIC
L/87

-------
la
SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: Las. U h E"E\
1 O L-\

FORM r SV-L
1/8 7 Rev.

-------
1C
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE .
i
:  0 (c) fluoranthene	
—aenzo(a)pyrene
—Indeno(1.2.3-cd)pyrene,
—Oibenz (a,h) anchracene__
—3enzo(g,h,i)perylene	

C>
3 2<20.
3 2.acJ
AJz&.

^•2.0 0
oSO
-~L-
% -2-££>


f.&e
JJZJ2
it-
±
tz
T-	i

1) - Cannoc be separacea :ran Dipnenylamine
"OFW I SV-2
L/87

-------
IF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE HO.
;	& hfz. d	Contract:; 6> %\
No. i tk&tkJ SAS No.: 	
Cass
Lab Name
f^ah Code:
Matrix: (soil/water) 66IL
Sample vt/vol:	3 6 (g/aL)	
Level: (lov/med) t-d Ia/
% Moisture; not dec. g."-,2_ dec.
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N)	P«:	
SDG Ho.;
Lab Sample ID: If/7*/
Lab file ID:
Date Received: ~1 i"2 b )*%>
Date Extracted: 7/27/37
Date Analyzed:
Dilution Factor: / i &
Number TICs found:
CONCENTRATION UNITS:.
(ug/L or ug/Kq)
CAS NUMBER
1.
2."
3/
4
5."
5."
7."
8."
9."
10."
12."
13."
14."
15."
16."
17."
18."
19."
20."
21..
22.
23."
24 .*
:s."
26."
27."
28."
23.
20.'

I
COMPOUND NAME
RT

i (J A/X,i/a w a/
	I
I E4hA»&. J. J,zy^-TTt 4eA I
I U .is 4 jV o as
I tJ <1 J A/a /\S
W A?M st/C i.!/££_ 4-*-;«/'	
6'7 5
I

EST. COMC.
ilea
tU£L
(,64.
I eJk,Z£
jj±o_
23JL
2. ¦V/^
2.d

?/.V9 I 2*>/gQ
Z25Z.
FORM I SV-TIC
1/87 Rev.

-------
13
SEMIV0LATIL2 ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: Lc.c. U h	•—/j=r ^ dl- Contract3—?2*r*7 |
Lato Coda: 	 Cas* Ho.:	1ahJs*S No.: 	 SDG Ho.:
P7.;r
1
Matrix: (soil/water) tkT (U
Sample vt/vol:	30-0 (q/aL)
Level: (lov/med) LC ^
% Moisture: not dec.£ ,7 dec.
Extraction: (SepF/Cont/Sonc) ^d)A/
-------
1C
SEMIVOLATILE ORGANICS ANALYSIS DATA SHE5T
EPA SAMPLE NO.
Lab Name
Lab Code
:	hContract: -&3^ \ P* ^
No.
Case
y*L
pH:
; 	 SDG No.: 	
Lab -Sample ID: 75/Q3
Lab File ID:	S ~2-
Date. Received: WW??
Date Extracted: 7/27/3 ?
Date Analyzed: ^)2-k
Dilution Factor: • \
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/Kq) U /^ /K(r- Q
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-	6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0—	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0—	
205-99-2	
207-08-	9	
50-32-8	
193-39-5	
53-70-3	
191-24-2	
—3-Hitroaniline
—Acenaphthene
-2,4-Dinitroptienol_
- 4 -N i tr ophenol	]
-Dibenzofuran
—2,4-Dinitrotoluene_
—Diethylphthalate_
—4 -Chloropheny 1-pheny lether	
—Fluorene
—4-N itroaniline	
-4,6-Dinitro-2-methylphenol	
-H-Nitrosodiphenylamine (1)	
-4-Bromopheny1-phenylether	
—Hexachlorobenzene	
—Pentachlorcohenol
—Phenanthrene	
—Anthracene
—Oi-n-butylphthalate_
—Fluoranthene	~
—Pyrene
—Butylbenzylphthalate	
—3,3*-D. ilorobenzidine
—8enzo(a nthracene	
Chrysene
—bis(2-Ethylhexyl)phthalate_
—Qi-n-octylphthalate	\
—3enzo(b)fluoranthene	
—3enzo()c) fluoranthene	
—3enzo(a)pyrene
—Indeno(1,2,3-ed)pyrene
•—Oibenz (a, h) anchracene_j
—3enzo(g,h,i)perylene	
-3,-2.0 0
±Ji_C_


&
C
c
~ -> s. c
i 6 a


£6 a
2
IjSL

_2_2.
jL££L
1) - Cannot be separated from OLpnenylamine
o

37*
FORM I SV-2
1/87 Rev.

-------
IF
SEMIVOIATILE CRGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE J »
Lab Name: L £>*- K — E"'6
Contract:-&3"32ft*? I f* *7/
Lab Cade:
Case Ho.:.40*/%/iU*S M
Date Received: 7/25/5^
Date Extracted: "7
Date Analyzed: 7 /2 /& 9
I O
Dilution Factor: / f
Nuaber TICs found:
CONCENTRATION UNITS:
(ug/L or nq/Kq) Je¥ /fOj
CAS NUMBER
COMPOUND NAME
1.
2."
3
4	•
s.~
6.""
7."
8."
9 . ™
10."
11."
12."
13."
14."
15."
16."
17."
18."
19."
20."
21."
22."
23."
24 .
25.'
26.
27.
*"* O
40'
29.
30.
*>
I J fiJ i< ,"J C uJ A/
<5,3 7
e+tsm* K/.2.1,- te+dAt.+.Jre*	I
U A/<'»**> 4/	I <=> .£'¦*>
-J *J	I *f.*7
7^
2 ?.-S V
7 /. f 7
T?',y 2
^
? 6
r/ a
11 ssat

7. 0£_0
n>i
Q-&
' 1C &
FORM I SV-TIC
1/87

-------
IB
SEMTVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name:
Lab Code:
L&4.U. h&sd —	Contract*7 | f* ^ 3	|
	 Case No.	Jsas No.: 	
Matrix: (soil/water)
Sample vt/vol:	30>Cj (q/aL) &•
Level: (lov/ned) Ld^/
% Moisture: not dec. // *7 dec. 	
Extraction: (SepF/Cont/Sonc)
(VN)Jli	pH:.
*70 "J&
G?C Cleanup:
CAS NO.
COMPOUND
	 SDG No.: 	
Lab Sample ID: 95/ £ *2*
Lab File ID: y	>
Date Received:
Date Extracted: 7/2.-y/g?
Date Analyzed:
Dilution Factor: / > ^
CONCENTRATION UNITS:
(ug/L or uq/Kq)
108-95-2	
—Phenol
111-44-4	
—bis(2-Chloroethyl)ether
1
1
1
1
1
1
1
CO
l
r-
m
1
m
0*
—2-Chi0rooheno1
541-73-1	
—1.3-Dichlorobenzene
106-46-7	
—1.4-Dichlorobenzene
100-51-6	
—Benzvl alcohol
95-50-1	
—1.2-Dichlorobenzene
95-48-7	
—2-Methvlohenol
108-60-1	
—bis (2-Chloroisopropyl) ether
106-44-5———-4-Methylohenol
621-64-7	
—N-Nitroso-di-n-propylamine	
67-72-1	
—Hexachloroethane
98-95-3	
—Nitrobenzene
78-b9-l	
—Isoohorone
88-75-5	
—2-Nitrophenol
105-67-9	
—2.4-DimethylDhenol
65-85-0	
—Benzoic acid
111-91-1———bis (2-Chloroethoxy) methane
120-83-2	
—2.4-Oichlorootienol
120-82-1———1.2 r 4-Triehlorobenzene
91-20-3	
—Naphthalene
106-47-8——4-Chloroaniline
87-68-3	
—Hexachlorobutadiene
59-50-7	
—4-Chlaro-3-nethvlohenol
91-i 7-6	
—2-Methylnaphthalene
77-47-4	
	Hexachlorocvclopentadiene
88-06-2	
	2.4.6-Trichlorophenol
95-95-4	
	2. 4.5-Trichlorophenol
91-58-7	
—2-Chloronaphthalene
38-74-4	
	2-Nitroaniline
131-11-3	
—0imethylphthalate
208-96-8	
—Aeenaohthylene
606-20-2	
	2.6-0initrotoluene
'1C

J
kU.

G»~70

7>zac


zz:
FORM I SV-1
1/87 Rev.

-------
1C
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: h Contract:| 3
Lab Code:	Case No. -.^^g/W^SAS No.: 	 SOG No.: 	
Matrix: (soil/water)
Sample vrt/vol:	3Q>£> (g/mL)
Level: (low/med)
% Moisture: not dec, i> *~7 dec.	
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: CY/N) Y
CAS NO.
pH:
COMPOUND
Lab Sample ID: *7*5)
Lab File ID:	j
Date. Received: _V
Date Extracted: 7 /2.
Date Analyzed:	/3J
Dilution Factsr: / /
CONCENTRATION UNITS;
(ug/L or uq/K
	4 -Nitrophenol	]
	Dibenzofuran
——2,4-Dinitrotoluene_
——Diethylphthalace_
	4-Chlorophenyl-phenyletiier	
——Fluorene
——4-Nitroaniline	
	4, 6-Dinitro-2-metbylphenol	
——N-Nitrosodiphenylamine (1)	
——4-Bromophenyl-phenylether	
	—Hexachlorobenzene
——Pentacftlorophenol	
	Phenanthr ene	
-—-Anthracene
—— Di-n-butylphtiialate_
—-~rluoranthene	
		Pyrene
——Butvlbenzvlphtftalate
	3,3 *-D, ilorobenzidine
——3enzo(a ntiiracene	
•Chrysene
	bis(2-Ethylhexy1)pnttialate_
.—-—Di-n-octyiphthalate	
—	3enzo(b)fluoranthene	
	Benzo(k)fluorantftene	
	3enzo(a)pyrene
	Indeno(1,2,3-cd)pyrene_
	Dibenz(a,h)anthracene_
——Benzo (g,h,i)perylene	
5-za>0
<2
i "z.a a

U7#
zee

fe 70
±:

A

2.
a
24 0

t,r £>
_=k.
t ?c><
•-iV
LTTO
U
m
u
z;
1) - Cannot be separated from Dipnenylamine
FORM I SV-2
1/87

-------
IF
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name
Lab Coda:
: Lac-k. h jEfJ ~	Contract:2\	^ ^ 3
i
______ Case No. : McF/tfl+rJ SAS No.: ^____
SDG No.:
Matrix: (soil/water
Sample wt/vol:	3 £ (q/mL) 6-
Level: (lov/med) Lfi IaJ
% Moisture: not dec. /1 "7 dec.	
Extraction: (SepF/Cont/Sonc) 1
G?C Cleanup: (Y/N)^	pH:	
Number TICs found: 	
Lab Sample ID: ^ 5 f h ^
Lab File ID: J(-*?£-*•/ "Z
Date Received: T f"2.
Date Extracted: -rhsftl
Date Analyzed: Izf/gj
Dilution Factor: ),Ci
CONCENTRATION UNITS: ,
(ug/L or uq/Xq) UL-IK&"
CAS NUMBER
COMPOUND NAME
1.
2."
3."
4 .""
5."
6."
7."
8."
a # ~"
10."
11."
12."
13."
14."
15."
16."
17."
18."
19."
20.
21."
22."
23."
24 ."
25."
26."
27.'
28.'
29.'
20.'
I U a/ fZ. AS £ taJ n/.
'l J * sU.l uf a/
—	IU V rt.x'Q «J V HYDhtC CA *'/?/" *J<
J=	riYi \ 6C AfigP.V

\	i.t.l.L. 1Vr*.'//-Vr
— I V
— I vWK,Vaw/l/

\u,y < Mow/y
		1	Xnet iSA/
LJ »e3 us t/
' 	I iJ ** k	Hei-a-vi?
r-j—
— 1U**/ n a »"i/ h)\,J£oc*
— I U-^k.
=	I ,)a/X.a/j^A/
	 \ OAfK.lAnxj/A/	A&&/V
_=	I uv  "¦

ZJ.
£L
2^23-
±d*.2.

EST. CONC.
t-fPQO

7- °
fj 
~5Zl.
oc
LA

-±L$JL
0 o
2. GCfi
! OM
(1M
l_r
FORM I SV-TIC
1/87 R«v

-------
13
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
I
: L k- h != — F~ Contract 7 "32V? I ^ ^ ^ ^
	 Case Ho.	Ia»J SAS No.: ______ SDG No.: 	
Lab Name
Lab Code:
Matrix: (soil/water) *50 L.
Sample vt/vol:	"3 C . C (q/aL) 6-
Lavel: (lov/med) c~£ W
dec.
% Moisture: not dec. 2-1 C		
Extraction: (SepF/Cont/Sonc) <:¦>!

1 t.7i3l

! \

1 fc
7 a i

1
!

i


1 -i— 1 -
¦ " !
FORM I SV-l
1/3 7

-------
1C
SEMXVOLATILE ORGANXCS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: L ££¦ MA £Contract	?—? "2*1*3 | } H/ ^7
i. >49e./^A khJs
Lab Code:
Case Ho.
'SAS No.
Matrix: (soil/water) li—
Sample vt/vol: 3£id (a/mL)
Level: (low/med) LC VJ
% Moisture: not dec. — > & dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N)_Y_	pH:	
	 SDG Ho.: 	
Lab Sample ID: ^ ^ / z7"
Lab File ID:
CAS NO.
COMPOUND
Date. Received: -rhztef
Date Extracted: -r/*r/a?
Date Analyzed: ^/2/g?
• Dilution Factor: /, £
CONCENTRATION UNITS;
(ug/L or uq/Kg)U6-iKc- Q
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-	6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-3	
193-39-5	
53-70-3	
191-24-2	
¦3-Nitroaniline_
•Acenaphtiiene_
¦2,4-Dinitrophenol_
¦4 -Hitrophenol	~
¦Dibenzofuran	
¦2,4-Dinitrotoluene_
»Diethylphthalate_
•4-Chlorophenyl-phenyletiier	
•Fluorene 	
-—4 -Hitroaniline
—4,6-Dinitro-2-inethylphenol	
—N-Nitrosodiphenylamine (1)	
—4-3roaophenyl-phenylether	
—Hexachlorobenzene	
—Pentachlorophenol	
—Fhenanthrene	
—Anthracene	
—Di-n-butylphtiialate_
'-Fluorantftene
—Pyrene_
—Butylbenzylphthalate	
—3,3'-D. -tlorobenzidine_
—Benzo(a anthracene	~
¦Chrysene_
—bis(2-Etiiylftexyl) pntftalate	
—Oi-n-octylphtftalate	
—3enzo(b) fluorantftene	
—3enzo(Jc) fluorantftene		
—3enzo(aj pyrene_
-Indeno(1,2.3-cd)pyrene_
-Dibenz(a,ft)anthracene_
	3enzo(g,h,i)perylene	

6 yo


b~r c
¦1 •*£<£>


hip
J3j£L.
9 ?. °
-f-

ft 7 a
O
—
±
-------
IF
Lab Naae: L6&
Lab Code: 	
SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
k b&mJ Lz^p £-¦
Contract: 63~0}~s'21'J
Case No. •.AUQfljj**SAS No.: _____ SDG No.
Matrix: (soil/water\
Sample vt/vol:	1 £) (g/»L) u-
Level: (low/aed) LC
i Moisture: not dec. Z. rO dec.	
Extraction: CSepF/Cont/Sonc)
G?C Cleanup: (Y/N) Y	pH:	
Number TICs found:
EPA SAMPLE
/£ J J"
*> i> / 7 J
Lab Sample ID:
Lab File ID: 7* t~*?
?«
Date Received: "7 Iz£'/'3
Date Extracted: "7h.7/jj|
Date Anaivsed: 9/2./$/
Dilution Factor:
/ r £
CONCENTRATION UNITS:
(ug/L or ug/Kq) (j j K J < J
1 (? rb f, / , i, ?, • 7f n /a fie
1 CJ V* A/ J saJ/1/
1 "5 : I
1 9,23 1
<*e n 1
*>W£>0 1

1 J 4/mT si/? u//1/"
1^.6 7 1
6 Z1* 1

\t/ S/ J si*,-? wt/ -^1/
1 >4/ !
'T2<5 1

1 U */ K A/ J M/ 4/
1 ftf.Vv 1


1 i/ V K 4/ */ /v' * -* ^8# -V
1 !
^ t—/ /"*

1 ijy c k>(? -^is
i ?'/ !
a "-5^

yj-V !>/V td*y,J )0*. 1/
1 ZI./.4 1

m
\Um/ iS» rJ~c/la* as
122,^ f

m
\() 1/ha a/~ A/us. A-/i.&30AJ
\ZJ,A<5 1
* 0 c
.
1 -J kt nrfuv a/
I L*->,e*7 1

•
1 U «J Kt h s m/ A/
\Z 1
7
*

1 ^"9 1
*=f  a w ~!/
I2"5,^X

•
1
J ' .1

«
1 £/  £" I
7, Kxn
.
1 Ui/>{)*<> n/"V
\3/,JI
L
.

1 1?,??
2

1 £/*/ kL»s) .i/Af V iJ/*
! ?V,2*7

1 II
I 1 \
1 1 1
1 1 1
J.
|
I
ii
I
1
FORK I SV-TIC
1/8

-------
6B
SEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name:LOCKHEED-ESC	Contract:68-03-3 249
Lab Code: 	 Case No.: MSthiizUolsAS No.: 	 SDG No.:
Instrument ID: 70 2 Calibration Date(s): 8/z&?/89 	
Min RRF for SPCC(#) ¦ 0.050	Max %RSD for CCC(*) = 30.0%
LAB FILE ID:
RRF80 =>LSC03
RRF20 =>LSC01
RRF120=>LSC04
RRF50 =>LSC02
RRF160=>LSC05
COMPOUND
Phenol	
bis(-2-Chloroethyl)ether	
2-Chlorophenol
1.3-Dichlorobenzene
1.4-Dichlorobenzene
Benzyl_alcohol	|
1,2-Dichlorobenzene
2-Methylphenol
bis(2-chloroisopropyl)ether
4-Methylphenol	
Hexachloroethane_
Nitrobenzene	~
Isophorone_
2-N itrophenol ~
2, 4-Dimethylphenol_
Benzoic acid
bis(-2-Chloroethoxy)methane
2,4-Dichlorophenol	
1,2,4-Trichlorobenzene
Naphthalene^	
4-chloroaniline
Hexachlorobutadiene
4-Chloro-3-methylphenol,
2-Methylnaphthalene
2,4,6-Trichlorophenol_
2,4,5-Trichlorophenol~
2-Chloronaphthalene	~
2-Nitroaniline	
Dimethyl Phthalate
Acenaphthylene_
2,6-Dinitrotoluene
3-N itroan i1ine	
Acenaphthene
2,4-Dinitrophenol.
4-Nitrophenol	[
RRF20
RRF50
RRF80
RRF120
RRF160
RRF
RSD

sasssa
sassasss
======
======
======
sssssa
sssss
*
1.2133
1.2523
1.3361
1.3274
1.
2315
1.2721
4 . 42C

1.31
1.2807
1.3412
1.1696
1.
1865
1.2576
6.038

0.9251
0.9065
0-.9602
0.9344
0.
9055
0.9264
2.436

1.2839
1.1469
1.164
0.9957
1.
0565
1.1294
9. 757
*
1.3065
1.1074
1.1229
1.0289
1.
0719
1.1275
9.437

0.242
0.4449
0.4611
0.5035
0.
5527
0.4408
26.93

1.2721
1.1143
1.0649
0.9011
0.
9801
1.0665
13.21

0.7908
0.8231
0.886
0.8022
0
.844
0.3292
4.547

2.2828
2.1638
2.3839
2.1857
2.
2711
2.2575
3.382

0.6825
0.7372
0.7392
0.6925
0.
7408
0.7184
3 .966

0.738
0.8244
0.895
0.8413
0.
9263
0.845
8.574

0.592
0.4945
0.4949
0.4439
0.
4689
0.4988
11.26

0.3612
0.3697
0.3377
0.3332
0.
4019
0.3607
7. 672

0.6545
0.663
0.6734
0.6687
0.
7545
0.6828
5.956
*
0.131
0.1604
0.1641
0.1695
0.
1708
0.1591
10.23

0.1901
0.2194
0.2324
0.2164
0.
2314
0.2179
7.358


0.1531
0.201
0.2225
0.
2538
0.2076
20 . 33

0.3947
0.3997
0.4219
0.4307
0.
4307
0.4159
4 . 1391
*
0.1749
0.2167
0.2221
0.2192
0.
2374
0.2141
10.39)

0.3068
0.2815
0.274
0.2528
0
•364
0.2758
7.-104)

0.85
0.7926
0.7463
0.7769
0.
707 J
0.7746
6.385)


0.0321
0.0526
0.0553
0.
0605
0.0501
24 .37)
*
0.19
' 0.1743
0.1618
0.1589
0.
16041
0.1691
7.311
*
0.1972
0.2316
0.262
0.2712
0.
2388
0.2502
14 .45

0.5086
0.4485
0.43591
0.4096
0
.466
0. 45371
3. 139
# 0.4533
0.5313
0.4964
0.4868
0.
4907
0. 4917
5 . 555
*
0.3566
0.4171
0.41471
0.4205
0.
4109
0.4039
6. 615

0.3696
0.4213
0.3884
0.3944
0.
4195
0.3986
5 . 484

1.167
1.1401
1.1002
1.0088
1.
0994
1.1031
5.432

0.1855
0.3537
0.4145
0.422
0.
419?
0.3588
28 . 11

1.25221
1.2774
1.2769
1.2015
1,
29$?
1.2429
2.982
1.3624
1.3545
1.2608
r1.1571
1,
1469
1.2563
a.225

0.2575
0.319
0.3133
0.3214
o,
3464
0.3115
10.52


0.1059
0.1327
0.1313
0.
131?
0.1'.53
10. 34
*
1.1439
1.1331
1.0567
1.0357
0.
9803
1.07
6.417
#

0.1466
0.1996
0.2096
0.
2243
0. 199
17 . 33
#

0.2087
0.312
0.3366
0.
3723
0.3074
22 .88








FORM VI SV-1
1/87 Rev.

-------
6C
SEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name:LOCKHEED-ESC	Contract:68-03-3249
Lab Code: 	 Case No.:	SAS No.: 	 SDG No.: 	
Instrument ID: 70 2 Calibration Date(s) : 0>/zi*lQQ 	
Min RRF for SPCC(#) = 0.050	Max %RSD for CCC(*)
LAB FILE ID:
RRF80 =>LSC03
RRF20 =>LSC01
RRF120=>LSC04
RRF50 =>LSC02
RRF160=>LSC05
COMPOUND
Dibenzofuran
RRF 20
1.5931
RRF50
1.5218
RRF80
1.4534
RJRF120
RRF160
RRF
1.4008
1.4955
1. 4929
2,4-Dinitrotoluene
0.302
0.3971
0.4203
0.433
0.4501
0.4005
Diethylphthalate
1.3304
1.2258
1.229
1.1073
1.1178
1.202V
4-Chlorophenyl-phenylether_
Fluorene
0.5989
0.6183
0.6152
0.5358
0.5458
0.5328
1.2003
1.1494
1.0363
1.0155
0.9713
1. 0747
4-Nitroaniline

0.0943
0.1641
0.1702
0.1738
0.1506
4,6-Dinitro-2-methylphenol_
0.0551
0.1009
0.1196
0.1212
0.1209
0.1035
N-Nitrosodiphenylamme (l) *0.3 334
0.3581
0.36
0.3439
0. 349
0.3489
4-Bromophenyl-phenylether	
Hexachlorobenzene
0.1803
0.1945
0.1925
0.1834
0. 192
0. 1336
0.2845
0.2751
0.2769
0.2597
0.2669
0.2726
Pentachlorophenol *0.1165
0.1508
0.1643
0.1616
0.1698
0.1526
Phenanthrene
0.7569
0.7599
0.7587
0.7009
0.7421
0.7437
Anthracene
0.7294
0.7118
0.6844
0. 666
0.6952
0.6973
Di-n-Butylphthalate
0.9306
0.9503
1.0459
0.9653
0.9875
0.9759
Fluoranthene * 0.737
0.7567
0.7593
0.7294
0. 747
0.7459
Pvrene
1.4074
1.2546
1.3203
1.2458
1.3474
1.3151
Butylbenzylphthalate
0.6198
0.6362
0.6867
0.7022
0.7348
0.6759
3,3'-Dichlorobenzidine

0.1052
0.1487
0.1714
0.1417
0.1417
Benzo(a)anthracene
0.9169
1.0358
1.0232
1.0456
1.1088
i. 02 6
Chrvsene
1. 139
1.0124
0.8974
0.9296
0.9663
0.9889
bis(2-Ethylhexyl)Phthalate
0.857
0.8852
0.8971
0.8885
0.9333
0.3922
Di-n-octyl phthalate *2.2198
2.012
2.1122
2.1116
2.2247
2 . 136
Benzo(b)fluoranthene
1.2125
1.6391
1.4959
1.6667
1.7576
1.5544
Benzo(k)fluoranthene
1.6119
1.0526
1.2964
0.977
1.1303
1.2136
Benzo(a)pyrene *1.0893
1.1023
1.1353
1.1132
1.1729
1.1226
Indeno(1,2,3-cd)pvrene
0.7431
1.2156
1.3121
1.3899
1.3413
1. 2004
Dibenzo(a, h)anthracene
0.3712
0.8691
1.0111
1.0782
1.1889
0.9037
Benzo(g, h,ijpervlene
0.7787
1.0714
1.1404
1.1802
1.2587
1.0859
Nitrobenzene-d5
nasaaa:
0.314
aaaaaaa:
0.3577
0.3764
0.3723
0.3891
0.3619
2-Fluorobiphenyl
1.274
1.3383
1.2468
1.185
1.2129
1.2514
Terphenyl-dl4
0.9751
0.9354
1.0207
'0.9431
0.9876
0.9724
Phenol-d5
0.4947
0.5084
0.5928
0.566
0.5913
0.5506
2-Fluorophenol
0.7803
0.8469
0.8856
0.7783
0.8503
0.8283
2,4,6-Tribroraophenol
0.1323
0.1572
0.1703
0.1591
0.1657
0.1569







I
I
5
I
(1) Cannot be separated from Diphenylamine
FORM VI SV-2
l/sa

-------
6B
SEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name:LOCKHEED-ESC	Contract:68-03-3249
Lab Code: 		 case No. ://lc/ru>WJsAS No.: 	 SDG No.: 	
Instrument ID: 70 2 Calibration Date(s) : fi/gn/gq 	
Min RRF for SPCC(#) = 0.050	Max %RSD for CCC(*) = 30.0%
LAB FILE ID: RRF20 =>LSC61
RRF80 =>LSC63 RRF120=>LSC64
RRF50 =>LSC62
RRF160=»>LSC65



COMPOUND
RRF20
RRF50
RRF80
RRF120
RRF160
RRF
RSD
Phenol
kl. 7493
1.7747
1.6817
1.3648
1.
2752
1.5692
14.79
bis(-2-Chloroethyl)ether	
1.6487
1.7059
1.4536
1.2611
1.
2324
1.4603
14.82
2-Chlorophenol
1.2139
1.2477
1.0541
0.9944
0.
9961
1.1012
11. 01
1,3-Dichlorobenzene
1.3524
1.2722
1.0354
1.0571
1.
0238
1.1482
13.32
1,4-Dichlorobenzene *1.2734
1.3068
1.0935
0.8803
0.
9282
1.0965
17.69
Benzyl alcohol
0.4924
0.7127
0.6674
0.6825
0.
6431
0.6396
13.45
1,2-Dichlorobenzene
1.3703
1.1984
1.0548
0.9928
0.
9187
1. 107
16.21
2-Methylphenol
1.1788
1.2173
1.0463
0.9788
0.
9672
1.0777
10.65
bis(2-chloroisopropyl)ether
3.0306
3.1959
2.9589
2.5884
2.
1978
2 .7943
14 . 34
4-Methylphenol
1.2683
1.1793
0.9305
0.9851
0
.986
1.0698
13 . 62
N-Nitroso-di-n-propylamine_i
rl. 1445
1.1572
1.1452
0.6265
0.
6507
0.9448
29.60
Hexachloroethane
0.609
0.5902
0.5201
0.4881
0.44
0.5295
13.29
Nitrobenzene
0.4144
0.4285
0.3997
0.4565
0.
4238
0.4246
4 . 940
Isoohorone
0.8164
0.895
0.8434
0.8517
0.
8136
0. 844
3 .908
2-Nitrophenol *0.1691
0.1821
0.1769
0.186
0.
1775
0.1783
3.556
2.4-DimethvlDhenol
0.2595
0.2688
0.2484
0.2638
0.
2635
0.2608
2.943
Benzoic acid
0.1327
0.2126
0.0713
0.0602
0.
0391
0.1032
68 .20
bis(-2-Chloroethoxy)methane
0.4733
0.5036
0.4885
0.5033
0
.468
0.4873
3 .336
2.4-Dichlorophenol *0.2447
0.2626
0. 23
0.175
0.
1828
0.219
17 . 53
1,2,4-Trichlorobenzene
0.2783
0.2645
0.2502
0.2381
0.
2438
0.255
5 .404
Naphthalene
0.8785
0.779
0.7372
0.6336
0.
4736
0.7004
22 . 02
4-Chloroaniline
0.0842
0.1263
0.1316
0.0965
0
.068
0.1013
25.9
Hexachlorobutadiene *o.1564
0.1472
0.1437
0.1205
0.
1173
0 . 13 7
12.56
4-Chloro-3-methylphenol *0.3119
0.3431
0.3088
0.3213
0.
3299
0. 323
4 . 316
2-Methvlnaphthalene
0.485
0.515
0.4395
0.4828
0.
4315
0.4708
7 . 377
Hexachlorocyclopentadiene #0.3502
0.3422
0.3357
0.3017
0.
3002
0.326
7. 194
2,4,6-Trichlorophenol *0.4128
0.3929
0.3359
0.403
0.
3905
0. 397
2.723
2,4,5-Trichlorophenol
0.413
0.4582
0.4101
0.386
0.
3388
0. 4012
10.85
2-Chloronaphthalene
1.228
1.1649
1.0231
1.0251
0.
9347
1.0752
11.04
2-Nitroaniline
0.4433
0.513
0.5381
0.5242
0.
5254
0.5088
7 . 404
Dimethyl Phthalate
1.4498
1.3802
1.2475
1.1352
1.
1122
1.265
11.71
Acenaphthylene
1.425
1.2512
1.0372
0.986
0.
8717
1.1142
19.39
2.6-Dinitrotoluerie
0.35
0.3786
0.3175
0.3156
0
.334
0.3392
7 . 688
3-Nitroaniline
0.1999
0.2137
0.2154
0.1953
0.
1448
0.1938
14.82
Acenaphthene *1.2157
1.0578
1.0794
0.9521
0.
9226
1.0455
11. 12
2.4-Dinitrophenol #0.0964
0.1702
0.1678
0.1941
0.
2086
0.1674
25.78
4-Nitrophenol #0.3211
0.4363
0.4298
0.4568
0.
4721
0.4232
14 . 05








FORM VI SV-1
1/87 Rev.

-------
6C
SEMIVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name:LOCKHEED-ESC	Contract:68-03-3249
Lab Code: 	 Case No.	SAS No. : 	 SDG No. :
Instrument ID: 70 2 Calibration Date(s) ¦atom 	
Min RRF for SPCC(#) = 0.050	Max %RSD for CCC(*)
LAB FILE ID: RRF20 =>LSC61 RRF50 =>LSC62
RRF80 =>LSC63 RRF12 0=>LSC64 RRF160->LSC65
COMPOUND
RRF20
RRF50
RRF80
RRF120
RRF160
RRF
Dibenzofuran
1.7314
1.7055
1.4672
1.3655
1.208
1.4955
2,4-Dinitrotoluene
0.4928
0.5283
0.4701
0.474
0.4957
0.4922
Diethvlphthalate
1.4068
1.3682
1.19831
1.013
0.6562
1.1285
4-Chlorophenyl-phenylether_
Fluorene
0.6277
0.5669
0.5179
0.3774
0.342
0.4864
1.2468
1.0464
1.009
0.3889
0.3645
1.0111
4-Nitroaniline
0.1811
0.1992
0.206
0.2083
0.2654
0. 2121
4,6-Dinitro-2-methylphenol_
0.0802
0.1034
0.0996
0.0909
0.0905
0. 0928)
N-Nitrosodiphenylamine_(l)_j
4-Bromophenyl-phenylether	
Hexachlorobenzene
* 0.4001
0.3806
0.3756
0.3379
0.3156
0. 3619
0.183
0.1763
0.158S
0.1521]
0.1534
0.1647
0.2565
0.2283
0.2322
0.1953
0.2125
0.2249
Pentachlorophenol *0.1381
0.1485
0.1514
0.1276
0.1365
0.1404
Phenanthrene
0.8033
0.7258
0.7396
0.6493
0.6254
0.7087
Anthracene
0.7963
0.6834
0.6679
0.5653
0.5121
0. 645
Di-n-Butylphthalate
1.1821
0.9444
0.8827
0.6961
0.5875
0.3586
Fluoranthene *0.8173
0.7404
0.6784
0.6318
0.5716
0.6879
Pyrene
1.6145
1.8369
1.7038
1.6005
1.6232
1.675S
Butylbenzylphthalate
0.9026
1.0389
0.928
0.9048
0.3991
0. 93471
3,3'-Dichlorobenzidirie
0. 24461
0.2032
0.2045
0. 141
0.130U
0. 13 4 5!
Benzo(a)anthracene
1.0989
1.1617
1.147
1.1164
1.1333
1. 13141
Chrysene
1.0903
1.0498
1.0234
0.9536
1.0391
1.0313
bis (2-Ethylhexyl) Phthalate_
1.1488
1. 188
1.1717
1.0936
0.9886
1.1181
Di-n-octyl phthalate
* 2.6729
3.3048
3.0626
2.1694
1.9693
2.6358
Benzo(b)fluoranthene
1.2771
1.4481
1.6644
1.8086
0.9953
1.4387
Benzo(k)fluoranthene •
1.4501
1.4753
1.1151
0.9286
0.9953
1.1929
Benzo (a) pyrene *1.1381
1.1797
1.1722
1.1039
1.1369
1.1461
Indeno(1,2,3-cd)pyrene
1.1854
1.0726
1.1641
1.1528
1.1729
1.1496
Dibenzo(a, h)anthracene
0.91491
0.8407
0.9255
0.92681
0.918
0.9052
Benzo(g,h,i)perylene
0.9705
0 .85181
0.9412
0.8964
0.9129
0.9146
Nitrobenzene-d5
0.4061
0.4324
0.45151
0.45271
0.42671
0.43391
2-Fluorobiphenvl
1.3139
1.28351
1.1526
1.12
0.9969
1.1734
Terphenyl-dl4
1.1389
1.2302
1.2156
1.1274
1.1542
1.1733
Phenol-d5
0.7614
0.7823
0 .70861
. 0.6876l
0.6512
0.7182
2-Fluorophenol
1.1471
1.043
1.0234
0.9729
1.0492
1.0471
2,4,6-Tribromophenol
0.1359
0.1332
0.1371
0.1262
0.1197
0.1304







r
jl 4;
¥
i|	
W
o .
r
it
t
•*.
-7
r
2.
r
4
f
1.
I
(1) Cannot be separated from Diphenylamine
FORM VI SV-2
1/87

-------
IB
SEMIVOLATILE ORGAHICS ANALYSIS DATA SHEET
IPA SAMPLE NO.
Lab Name: L ac U- h BB/J ~~ Contract;"32.^ I & )
Lab Code: ______ Case Ho.:rfLfcdAmJSAS Ho.: _____ SDG Ho.; __	
Matrix: (soil/water) f L.
Sample vt/vol:	l£,Q (g/mL) 6~
Level: (lov/aed) LdwJ
* Moisture: not dec. (9 ,S dec.
mmmmrnrn
Extraction: (SepF/Cont/Sonc> _____
G?C Cleanup: (Y/N) Y
CAS NO.
COMPOUND
Lab Sample ID: 5/46jQQ
Lab File ID: ?£-4£-/i
Date Received: 7/z-Jr
Date Extracted: 7/2jr/gf
. Date Analyzed: ±h£t&2
Dilution Factor: / r &
CONCENTRATION UNITS i ,
(ug/L or uq/Ka) tJA- / K*t <2
i
108-95-2—
111-44-4—
95-57-8—
541-73-1—
106-46-7 —
100-51-6—
95-50-1	
95-48-7	
108-60-1—
106-44-5—
621-64-7—
67-72-1	
98-95-3	
78-59-1—
88-75-5-
105-67-	9	
65-85-0	
111-91-1	
120-83-2	
120-82-1		
91-20-3	
106-47-	8	
87-68-	3	
59-50-7	
91-i 7-6	
77-47-4	
88-06-	2	
95-95-4	
91-58-7	
88-74-4	
131-11-3	
208-96-8	
606-20-2	
	Pheno1
—bis (2-Chloroethyl) ether.
—2-Chlorophenol_
1,3-0ichlorobenzene
	1,4-Dichlorobenzene
•—-Benzyl alcohol
—1,2-Dichlorobenzene
—2-Methylphenol
-bis(2-Chloroisopropyl5 ether_|
4-Methvlphenol	""i
N-N itroso-di-n-propylamine^ |
•Hexachloroethane	j
•Nitrobenzene	I
•Isophorone	I
¦——-2-Nitrophenol,
•—2,4-0imethylphenol_
•—Benzoic acid
bis (2-Chloroethoxy) methane,
2,4-Dichlorophenol.
...—i# 2,4-Trichlorobenzene
•Naphthalene
*4-Chloroaniline^	
-Hexachlorobutadxene
...4-chioro-3-methylphenol_
-2-Methylnaphthalene_
	Hexachlorocyclopentadiene^
	2,4,6-Trichloropheno1	[
	2,4,5-Trichlorophenol	
	2-Chloronaphthalene	
	2-Nitroaniline
		Dimethylphthalate_
	-Acenapftthylene	
—2,6-Oinitrotoluene
tod>£>\ J
,1 if 1.
ZZZjEZi,

"1

CJ





t
]/

-------
1C
SEMIVOLATILE ORG AN ICS ANALYSIS C.VTA SHEET
Lab Name: Ljc. h £p=tJ —
Lab Code: 	 Case No.:	No.:
EPA SAMPLE N
I
ContractI	$ /|
SDG No.
Matrix: (soil/water)
Sample vt/vol:	,0 (q/mL) 6~
Level: (low/med) l.0 yj
% Moisture: not dec. 0,0 dec.	
Extraction: (SepF/Cont/Scnc) SCS/Z-
V
Lab Sample ID: ^ *7 / is 6
Lab File ID: J>L.-eb£
J,

> 2&/>



1 ¦z.a#

JzJ=-J2-
V
1 o











































I «v.
1. T

1 V
1 r
1 1






1

! C,

(1) - Cannot be separated from Oipnenylamine

-------
IF
SEMTTOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO,
Lab Kane
Lab Coda
: ~ contract: 6$ 2 V*7 Jx
: 	 Case Ho. xAL&dj,*) SAS Ho.: 	 SDG Ho.: 	
Matrix: (soil/water)^I I—
Sample wt/vol:	~*)D, O fg/wL) &
Level: (low/ued) L-O W
% Moisture: not dec. iP >0 dec. 0 ,0
Extraction: (SepF/Cont/Sonc) 1djkr
GrC Cleanup: fY/N) V"
Lab Sample ID: MUM
Lab File ID: L J /
pH:
Number TZCs found:
Data Received: T /iM/S<^/'V/.4)
Date Extracted: 7 /^ £"/5^
Date Analyzed: ?/2-g/g^
Dilution Factor: /, <£)
CONCENTRATION OMITS;...
(ug/L or uqr/Xq) (J&!)<&-
CAS NUMBER
COMPOUND NAME
1.
2."
3."
4."
5."
6.
7.
I	H ynH.6t.Ait 6a «S
HY6 Ae&4.t/
I -i.tteT, n>re» e. Y«/.v h v a to* a a te>.*/
U4/K/V«ut4J H r 1	its*."/
a,
10."
11.'
12.'
14 ¦
15.
16.
17.
18.'
19.'
20.
21.
22."
23 ,
2 4 .
25.
26.
27.
13.
29.'
20.

	(*<*•'
\i/4/K A//9 J/aT
1 JaJKsVouJA,
-Tisrrfi A- £. AP>*et I

i/f K.





U A/ KL ASJU/A/



l/.l/KA/aii/A/




























COHC

2OQ
2ju2a
ZJZL2
/ y a
&2.0
nlk
LL*£A
a < f,
vTvX
E22

-------
IB
SEMIV0LATIL2 ORGANICS ANALYSIS DATA SHEET
Lab Mane: Lo~ ^^ /SlfJ —Contract: ^5 j~3 2
Lab Coda: .	 Case No. \
EPA SAMPLE

i
SAS No.:
SDG No.
Matrix: (soil/water) 4CT L
Sample vt/vol:	1 £ . 0 (q/mL)
Level: (lov/med) ^-<3  I


Q-J
H
I !

-------
1C
SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET
I
EPA SAMPLE NO.
Lab Name:	h FFsiContract:	I
Lab Code: 	 Case Mo.:	UtwJsAS No.: 	 SDG Mo.: 	
Matrix: (soil/water) ^>ClL^
Sample vt/vol:	(g/mLl
Lavel: (lov/med) U3UJ
% Moisture: not dec. CO ,£> dec.	
Extraction: (SepF/Cont/Sonc)
Lab Sample ID: *7 5 / ! Attfc
Lab File ID:
Date. Received: ~7
/2$/$7 (*'/*)
Date Extracted:
Date Analyzed:
G?C Cleanup:
CAS NO.
CY/N)
V
pH:
COMPOUND
Dilution Factsr:
CONCENTRATION UNITS.: /
(ug/L or ug/Kg)o6-JK&~
d
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-6—
534-52-1	
86-30-	6	—
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-3	
193-39-5	
53-70-3	
-3-Nitroaniline_
-Acenapfathene_
•2,4-Dinitrophenol_
•4-Hltroohenol
¦Dibenzofuran	
¦2,4-Dinitrotoluene
-Diethylphthalate_
-4-Chlorophenyl-phenylether	
-Fluorene	
——4 -Mitroaniline
-4,6-Dinitro-2-methylphenol	
-N-Nitrosodiphenylamine (l)	
—¦4-Bromophenvl-phenylether
—Hexachlorobenzene	
—Pentachlorophenol	
—Phenanthrene
—Anthracene
—Di-n-butylphthalate
—Fluoranthene	
—Pyrene
-9utylbenzylphthalate	
-3,3'-D. ilorobenzidine
-Benzo(a nthracene	
Chrysene
—bis(2-Ethylhexyl) pnthalate	
—Di-n-octylphthalate	
-,-3enzo(b) fluoranthene	
—3enzo(k)fluoranthene	
—Senzo(a)pyrene
—Indeno(1,2,3-cd)pyrene.
—Oibenz(a,h)anthracene
£>(>£
3
-3 2.^'
£ b C


h(jC
3
Z222
_£££L
iL

-------
IT
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE
Case Ho.	SAS No
Lab Name: / at. k h ggJ — £<£>
Lab Code: 	
Matrix: (soil/water) Sg? /
Sample vt/vol:	3 A (q/aL) £?-
Level: (lov/med) 2-<# k/
% Moisture: not dec. ^ dec.
Extraction: (SepF/Cont/Sonc
G?C Cleanup: (Y/N) Y'
Contract: 65 '31
I ^>&LK
af.
SDG No.:


Lab Sample ID: ^*5 / *7^31 *
Lab File ID:	S*
Date Received: xhiMj
Date Extracted: 1 )z7
Date Analyzed: /2-/*$
Dilution "actor: / , £
%
Number TICs found:
CONCENTRATION UNITS:.
(ug/L or ug/Xq) {J/r-fkC> /tj £ A/<3 v />j K 'V<5 w-/ A/
U K jYs> S*
RT

EST. COHC. |
i
-£
^ A*
s / ? H
%lk>
t£i7H
3
2_ Cj ?_
*72.6.
J±£i2.
• A
i i
o.

-------
IB
EPA SAMPLE MO.
SEMIVOLATILZ ORGAMICS ANALYSIS DATA SHEET		
I
Lab Name: Lctk kff&J —£ 	 Contract: 6% J| ^^ ^
Lab Code:
	 Contract:
Case No.: A^fituJsxs No.:
SDG No.
Matrix: (soil/water) *?£ f L.
Sample vt/vol:	3C.£ (q/mL} Q~
Level: (lov/med) /-/? m/
* Moisture: not dec. O < £> dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) V	pH:	
Lab Sample ID: f
Lab File ID:
CAS NO.
COMPOUND
Date Received: 71'ZfT/S^f S'V'/st)
Date Extracted:
Date Analyzed: ¦g/?//g9
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg)	Q
108-95-2	
111-44-4	
95-57-8	
541-73-1	
106-46-7	
100-51-6	
95-50-1	
95-48-7	
108-60-1	
106-44-5	
621-64-7——
67-72-1	
98-95-3	
78-S9-1	
88-75-5	
105-67-	9	
65-85-0	
111-91-1	
120-83-2	
120-82-1	
91-20-3	
106-47-	8	
87-68-	3	
59-50-7	
91-i 7-6	
77-47-4	
88-06-	2	
95-95-4	
91-58-7	
38-74-4	
131-11-3	
208-96-8	
606-20-2	
——Phenol
-bis(2-Chloroethy1)ether,
- 2-Chloropheno1_
•1,3-Dichlorobenzene_
¦1,4-Dichlorobenzene~
•Benzyl alcohol.
¦1,2-Dichlorobenzene_
»2-Methylphenol_
—bis(2-Chloroisopropyl)ether_
—4-Methyl phenol
—N-Nitroso-di-n-propylamine
—Hexachloroethane	
—N itrobenz ene	
—Isophorone	
	-2-Nitrophenol_
—2,4-0imethylphenol_
—Benzoic acid	"
—bis(2-Chloroethoxy)methane
—2,4-0ichlorophenol
—1,2,4-Trichlorobenzene_
—Naphthalene
——4 -Chloroaniline^	
——-Hexachlorobutadiene
—4-Chloro-3-methylphenol_
—2-Methylnaphthalene_
—Kexachlorocyclopentadlene	
—2,4,6-Trichlorophenol	
—2,4,5-Trichlorophenol	
—2-Chloronaphthalene	
—2-Nitroaniline	
—Dimethylphthalate_
—Acenaphthylene_
LLC \ O I
4-

3_2££l.
Ago |.
->>-ZCO
(,f>0
6 LP
—	2,6-Dinicrotoluene

!

:

1

I

J

1
FORM I SV-1
1/87 Rev.

-------
1C
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: Lac
Lab Code:
U b&E.d	ContractI ? ^ ^
	 Case No. x.Mtz/zjfiMhd SAS No.: 		 SDG Mo.: 	¦
Lab Sample ID: °}*5/ 37
Lab File ID: ">^ 5^. 7^
~ate. Received: *7 JS 7
Date Extracted:
Date Analyzed: <*,!?/J$?
• Dilution Factor: /; d-
Matrix: (soil/water) !L-
Sample vrt/vol:	1 Q,0 {<*/•&.L) (r
Level: (low/aed) L&W
% Moisture: not dec. 0,C> dec.	
Extraction: (SepF/Cont/Sone)
G?C Cleanup: (Y/N)	pH:	
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ucr/Kq) U£-JhX*— Q
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3—
86-73-7	
100-01-	6	
534-52-1'
86-30-	6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-0—
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218--01-9	
117-81-7
117-84-0	
205-99-2	
207-08-9	—
50-32-8	
193-39-5—
53-70-3	
191-24-2 —
	3-Hitroaniline
——Acenaphthene
	2,4-Dinitrophenoi
	4-Hitrophenol
-—Dibenzofuran
2,4-Dinitrotoluene_
	Dietiiylphthalate_
	^_
	4-Chlorophenyl-phenyl eerier	
	Fluorene
		4 -H itroan il ine	
		4,6-Dinitra-2-aetfcyipnenol	
	H-Nitrosodiphenylaaine (l)	
	4-Broaophenyl-phenyletiier	
——Hexacftlorobenzene
	Pentactiloroptienol	
	Phenanthrene	
-Anthracene
—	Di-n-butyipht&alate
	Fluoranchene	
	Pyrene
	rj4	mmm—mmrnmma—•
——— 3utylbenzylphtftalate	
—-—3 ,3 ' -D. -ilorobenzidine_
....—aenzo (a : ntiiracene	[
	Chrysene_
yaqnB
	bis(2-Etiiylr.exyl) phtnalate_
	Di-n-octylphthalate	
——3enzo(b) gluoranttiene
	aenzo (1c) fluoranctiene	
.——aenzo(a) pyrene
^ , p; -	
	Indeno(1,2,3-cd}pyrene
	Oibenz(a, h)anthracene^
	Senzo(g,n,i)perylene	
(1) - Cannot be separated iron Dipnenyiaoine
FORM I SV-2
"3 "2j£ C
'"6 G
1 2^*



*20 <-¦
6 Z- O

jJsJL
A.

mall
±.
f 1
-------
ir
SEMXVOIATILS ORGANXCS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
rzzx
Lab Name:.	Contract:
Lab Coda: _______ Case Ho. •.J^cSaIa>uJSAS No. :
Matrix: fsoil/water)
Sample vrt/vcl:	3 & (
Laval: (low/mad)
% Moisture: not dec. (9 & dac.	
Extraction: (SapF/Cont/Sonc) -fOtifC'
G?C Cleanup; (Y/N)	pH:	
EPA SAMPLE HO.
i5BU */ Ksvav*/
i
RT |
EST. CONC.
t.e'r~\~

•5 ijf 1
/ l&O
cf./4s i
o o

*~f €!£2
1,7/ I
3?6?
1
I
1
FORM I SV-TIC
i/87 Rev.

-------
IB
SEMIVOLATILZ ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
Lab Name: A 0c, k-	~2- £ — Contract: 6G~&')-32.'~t£7\ ^ F~^
Lab Code:
Case Ho.	SAS No.:
SOG Ho.
Matrix: (soil/water) <~>C>IL
Sample ve/vol:	(q/mL) d-
Lave 1: (1 ow/med) n/
% Moisture: not dec. /' / ^ dec.
Extraction: (SepF/Ccnt/Sonc) "tO V^~
GPC Cleanup: (Y/N)_2£_	pH:	
CAS NO.
COMPOUND
Lab Sample ID: $ f
Lab File ID: 7
Date Received:	5*/¦S'Tw
Date Extracted:
Data Analyzed: *5 j "2.S /
Dilution Factor: I ' &
CONCENTRATION UNITS: , . /
(uq/L or ug/Kg) o- !r^r~ Q
I 108-95-2	
--rhenol i
1 ) 1
£7^1 0 t
1 111-44-4	
—bis (2-Chloroectiyl) ether 1

!
i
! 95-57-8	
—2-Chloroohenol 1

1
!
I 541-73-1	
—1.3-Dichlorobenzene 1

1
1
1 106-46-7	
~1.4-Dichlorobenzene 1

1
1
I 100-51-6	
—Senzvl alcohol 1

1
1
| 95-50-1	
—1.2-Dichlorobenzene 1

1
1
| 95-48-7	
--2-Methylphenol 1

1
1
| 108-60-1	
—bis(2-Chloroisopropyl)ether 1

1
1
| 106-44-5	
—4-Methvlphenol 1

1
i
I 621-64-7	
—M-Nitroso-di-n-propylamme !

t

I 67-72-1	
—Hexachloroethane 1

1

I 98-95-3	
—Nitrobenzene 1

1

I 78-S9-1	
—Isoohorone 1

1

I 88-75-5	
—2-Nitroohenol 1

1

| 105-67-9	
—2.4-DimethvlDhenol 1

^ 1

1 65-85-0———Benzoic acid 1
^ I

| 111-91-1	
—bis(2-Chloroethoxy)netaane |
'a
*7 0 |

| 120-83-2		
—2.4-Dichloroohenol 1

1

I 120-82-1	
—1.2.4-Triciilorobenzene 1

. 1

I 91-20-3	
—-NaDhthalene 1

. 1

| 106-47-8	
	4-Chloroaniline 1

1

| 87-68-3	
-—Hexachlorobutadiene 1

n

| 59-50-7	
—4-Chloro-3-methylphenol 1

i

| 91-i 7-6	
—2-Methylnaphthalene I

i

| 77-47-4	
—Hexachlorocyclopentadiene |

i

I 38-06-2	
	2.4. 6-Tricftlorophenol 1

^ i

I 95-95-4	
	2. 4.5—Trichlorophenol 1
1 7 a d) \

I 91-58-7	
	2-ChlaronaohthaLene 1
C*~70 !

I 38-74-4	
	2-Ninroaniline !
^ yCCJ \

1 131-11-3	
-—Oiraetfiylphthalate 1
6 70 1

I 208-96-3	
—AeenaphtnvLene 1

i

I 606-20-2	
	2.s—oinicrocoluene _ 1




1

— i

FORM I SV-1
1/8 7

-------
1C
SEMIVOLATILE QRGANICS ANALYSIS DATA SHEET
Lab Name: L U h/rfirJ-	£*~
Contract: -c^-32^
EPA SAMPLE NO.
C i=-d) f
Lab Code:
case No. iJ'W^bft.Urd SAS No.:
SDG No.
Matrix: (soil/vater) ^/L.
Sample vt/vol:	3£ ,0 (g/mL)
Level: (low/med) ^.<2 tV
dec.
Lab Sample ID:	/>5"^
Lab File. ID:
% Moisture: not dec. /; ^
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: CY/N) V

pH:
Date. Received: 7
Date Extracted: _7/££/y
Date Analyzed:
Dilution Factor:
>r c
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg)	
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2	
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-	6	
101-55-	3	
118-74-1	
87-86-	5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-8	
193-39-5	
53-70-3	
191-24-2	
-3-Nitroaniline_
-Acenaohtfcene
•2,4-Dinitrophenol_
-4-Nitrophenol	
-Dibenzofuran
-2,4-Dinitrotoluene_
-0iethylphthalate_
-4-Chlorophenvl-phenyletter
•Fluorene
—4-Nitroaniline	
—4,6-Dinitro-2-meoylphenol	
—N-Nitrosodiphenylaaine (1)	
—4-aromophenyl-phenyletiier	
--Hexachlorobenzene	
—Pentachlorophenol	
—Piienanthrene_	
—Anthracene
--Oi-n-butylphthalate
—Fluoranthen*	
—Pyrene
—Butvlbenzvlphthalate
—3,3'-D. -.lorobenzidine
-Benzo(a ntiiracene	
—Ciirysene
-bis(2-Ethylhexyl)pntftalate	
—Oi-n-octylphthalate	__
—3enzo(b) fluorancnene		
— 3enzo(Jc) fluorancAene	
—3enzo(a)pyrene
-Indeno(1,2,3-cd)pyrene_
-Dibenz(a,h)anthracene_J
—9enzo(g,ft,i)perylene	


1-9(3 c


u
»<3 O I
2±GJ2-
<* ?c
-±r[
1 3
Ja2£L

JOjSL

7 £

i-J
51
u 1
1) - Cannot be separated from Oipnenylamine
FORM I SV-2
L/87 5

-------
IF
SEMIVOIATILZ ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAKPLB
:: jS '6 3-3^^1 ^ ^
Lab Name: L Jd, , - £/F^1'	Contract:
Lab Cade: 	 Case No.: 	 SAS No.: 	 SDG No.:
Matrix: (soil/water) **>£IL-
Sample vrc/vol: ?<£. (g/nL) 6~
Level: (low/med) U& ht
% Moisture: not dec. / r / dec.	
Extraction: (SepF/Cont/Sonc) e?C)/\/C~
GPC Cleanup: {Y/N)_Y_	pH:	
Lab Sample ID: ^ f ^
Lab File ID: L-*?£j
Date Received: *7 /
Date Extracted: ~7 12.
Date Analyzed:
Dilution Factor: / ,&
Number TICs Sound:
CONCENTRATION UNITS:.
(ug/L or ug/Kg) Ko-
CAS NUMBER
1.
2."
3."
4."
5.
6 •!
7.
8 •
a
I	10.
I	11.'
i	12.
I	13.
S	14.'
I	15.
I	16.
I	17.
I	18.
!	19.
t	20.
I	21.
I	22.
I	23.
!	24.
i	25.
I	26.
!	27.
1	23.
I	29.
I	20.
COMPOUND NAME
RT

.1 ^
I u*Jk?4J0 tf YD# A-/e Ga */l >, 6 /
\Ja/X«/4u/. /¦• C 1
3. / /?
FORM I SV-TIC

-------
IB
EPA SAMPLE NO.
SEMIVOLATILE ORGAMICS ANALYSIS DATA SHEET		
I
Lab Name: Lae-Ii-Contract :^S^-g^3-32.^*^ \ ^^
Lab Code:
Contract:
Case Ho. '.tfcBitkd SAS No.:
SOG No.:
Matrix: (soil/water)
Sample wt/vol:	G (q/mL) &
Level: (lov/aed)	bi/
% Moisture: not dec, i/ ^ dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N)	pH:		
CAS NO.
COMPOUND
Lab Sample ID:	J £ 4^
Lab File ID:	V 3
Date Received: ? /a-g/g?
Data Extracttd:
Date Analyzed:
Dilution Factor: / / 0
CONCENTRATION UNITS: .
(ug/L or ug/Kq) L'&lM6~ Q
108-95-2	
111-44-4	
95-57-8	
541-73-1	
106-46-7	
100-51-6	
95-50-1	
95-48-7	
108-60-1	
106-44-5	
621-64-7	
67-72-1	
98-95-3	
78-S9-1	
88-75-5	
105-67-	9	
65-85-0	
111-91-1	
120-83-2	
120-82-1	
91-20-3	
106-47-	8	
87-68-3	
59-50-7	
91-i 7-6	
77-47-4	
38-06-2	
95-95-4	
91-53-7	
38-74-4	
131-11-3	
208-96-3	
506-20-2	
——Phenol
¦bis(2-Chloroethyl)ether,
-2-Chlorophenol_
JzUi.
—
¦ 1,3-Dichlorobenzene_
•1,4-Dichlorobenzene"
•Benzyl alcohol.
6 74
"9-
¦1,2-Dichlorobenzene_
¦ 2-Methylpheno1_
67^
—bis(2-Chloroisopropyl)echerj^
—4-Methylphenol	~ |!
—H-Hitroso-di-n-propylamxne j"
—Hexachloroethane	|"
--N itrobenzene	|"
—Isophorone	| ]
—2 -N itropheno 1,	|'
—2.4-Dinethvlphenol 1
—Benzoic acid	i
1-
ZL
JC-
/iSe7.° '—LL
—bis (2-Chloroethoxy) methane	|
—2,4-Dichlorophenol	|.
—1,2,4-Trichlorobenzene	| _
—Naphthalene^	I'
—4-Chloroaniline	|



67,0
——Hexachlorobutadiene
—4-Chloro-3-methylphenol,
—2-Methylnaphthalene_
I

—Hexachlorocyclopentadiene	|
—2,4,6-Trichlorophenol	1
—2, 4 , 5-Trichlorophenol	
—2-Chloronaphthalene	1
—2-Nitroaniline	I
—Dimethylphthalate	I
—Acenaphthylene
U



-------
1C
.SEMJVOLATILE ORGAN ICS ANALYSIS DATA SHEET
EPA SAMPLE N.
Lab Name: L<9£-k bg&J «—*7^ Contract: £>4>-C'i \ C?/ d)//W^
_______ Case Mo.: /WcrfzdAnJ S AS No.: 	
Lab Code: _______
Matrix: (soil/water) *5Q)L^
Sample vt/vol:	£ (g/nL) 0~
Level: (low/aed) LfilV
% Moisture: not dec. /, ^ dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: CY/N)^£_	pH:	
SDG No.
CAS NO.
COMPOUND
Lab Sample ID:	¦
Lab File ID:
Date Received: 2j2£/2?
Date Extracted: /2^/
Date Analyzed:
Dilution Factor: /•&
CONCENTRATION UNITS.:
(ug/L or uq/Kg)UA-l)l6- Q
99-09-	2	
83-32-	9	
51-28-5	
100-02-	7	
132-64-9	
121-14-2	
84-66-	2		—
7005-72-3	
86-73-7	
100-01-	6	
534-52-1	
86-30-6	
101-55-	3	
118-74-1	
37-86-5	
85-01-	8	
120-12-7	
84-74-	2	
206-44-	0	
129-00-0	
85-68-	7	
91-94-1	
56-55-3	
218-01-9	
117-81-7	
117-84-0	
205-99-2	
207-08-	9	
50-32-8	
193-39-5	
53-70-3	
191-24-2	
- 3-N itroaniline_
-Acenaphthene_
-2,4-Dinitrophenol_
-4-Nitroohenol
-Dibenzofuran	
-2,4-Dinitro toluene,
-Diethylphthalate_
-4-Chlorophenyl-phenvlether
-Fluorene
—4-Nitroani1ine	
—4,6-Dinitro-2-methylphenoi	
—N-Nitrosodiphenylamine (1)	
—4-Bronophenyl-phenylether
—Hexachlorobenzene
—Pentachlorcohenol
—Phenanthrene	
—Anthracene
-Di-n-butylphthalate
—Fluoranthene	
—Pyrene
-Sutylbenzylphthalate
-3,3*-0. ilorobenzidine
-Benzo(a . nthracene	
-Chrysene
-bis(2-Ethylhexy 1)phthalate	
—Oi-n-octylphthalate		
—3enzo(b)fluoranthene
—3enzo(Jc) fluoranthene	
—Benzo(a)pyrene
—Indeno(1,2,3-cd)pyrene,
—Oibenz(a,h)anthracene	
—Benzo(g,h,i)perylene	
lied

blC
>-?c
_=J,

LLz£L

G



I


/1
1/
1
6 1£>
V
-L*
0-


t\~T A
U
I
(, ~7C
k)
) tae i

a in I
	
-L-
•s


U
IT



O'
i/
tK
U
*
u
u
1) - Cannot be separated from OLpnenylamine
FORM I SV-2
1/87

-------
IB
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
Lab Name: / *c.kh eeJ —		 Contract: ^-03-52 j
Lab Code:	Case No. '.AIcJ^a pj/i-njS AS No.: 	 SDG No
! crc i
_______ Case No. '.AIcJ^a S AS No.:
Matrix: (soil/water) ^^TZ.
Sample vt/vol:	(a/aL) 6~
Level: (lov/ned) L£ u/
% Moisture: not dec. /,	dec.	
Extraction: (SepF/Cont/Sonc) ^C-AJC.
G?C Cleanup: (Y/N) V	pH:	
Lab Sample ID: ^ "5 ( £ b
Lab File ID: ">L- V*7*
Date Received: '7/2.^/S^
Date Extracted: ~7 ) "2-57^*7
Date Analyzed: 5^/^^
Dilution Factor: /, ^
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/Kq) tjl"/£6-
108-95-2	
111-44—4	
95-57-8	
541-73-1	
106-46-7	
100-51-6	
95-50-1	
95-48-7	
108-60-1	
106-44-5	
621-64-7	
67-72-1	
98-95-3	
78-59-1	
88-75-5	
105-67-	9	
65-85-0	
111-91-1*	
120-83-2	
120-82-1	
91-20-3	
106-47-	8	
87-68-	3	
59-50-7	
91-i 7-6	
77-47-4	
88-06-	2	
95-95-4	
91-58-7	
38-74-4	
131-11-3	
208-96-3	
606-20-2	
-—Phenol
—bis(2-Chloroethy1)ether
—2-Chlo ropheno1	
—1,3-Dichlorobenzene
—1,4-Dichlorobenzene
—Benzyl alcohol	
—1,2-Dichlorobenzene
—2-Methylpheno1	
—bis(2-Chloroisopropyl)ether_
—4-Methy lpheno 1	~
—N-Nitroso-di-n-propylamine	
—Hexachloroethane
—Nitrobenzene
—Isophorone	
	2-Nitrophenol	
—2,4 - D ioethylpheno1
—Benzoic acid
-

—bis(2-Chloroethoxy)methane	
—2,4-Dichlorophenol	
—1,2,4-Trichlorobenzene
—Naphthalene_^	
	4-Chloroanilxne	
	Hexachlorobutadiene	
—4-Chloro-3-methylpheno i
—2-Methylnaphthalene	
—Hexachlorccyclopentadiene	
—2. 4, 6-Trichlorophenol
—2,4,5-Trichlorophenol
—2-Chloronaphthalene
—2-Nitroaniline	
—Oioethylphthalate
—Acenaohthvlene
	2,6-Oinitrotoluene
Al.+tfi.
6 70

-------
Lab Name
Lab Code
1C
SQ1IVOLATILE ORGANICS ANALYSIS DATA SHEET
: Lack- Us&d -/g	Contract:
	Case So. : /^/5^2-fAS No.: 	
EPA SAMPLE
O F- O I
4
SDG No.
Matrix: (soil/water)
Sample vrt/vol:	. C (q/mL) £r-
Level: (lov/med)
% Moisture: not dec. /¦ ^1 dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: CY/N)_^_	pH:	
Lab Sample ID: C1 *?[£b
Lab File ID:
Date. Received: Tr
Date Extracted: 7/S-'SV^lf
Date Analyzed:
Dilution Factor: ) , 
-------
IB
EPA SAMPLE i»0.
SEMXVOLATILZ ORGANICS ANALYSIS DATA SHEET			
I
Lab Name:	h (ZfrJ) ~	Contract:	I	^ ^
Lab Code:
?(?<& kZ-'-z>£,— Contract:
Case No.	SkS No.
SOG No.
Matrix: (soil/water) f?0 lL-
Sample wt/vol:	3O,0 (q/nL) 6~
Level: (lov/aed) I~£ IaJ
% Moisture: not dec. I« *7 dec.	
Extraction: (SepF/Cont/Sonc) /<£.
GPC Cleanup: (Y/N)_Y_	pH:	
Lab Sample ID: 95/06 ft &
Lab File ID:	<£-~7<£>
Date Received: t/s 4T i*o *7
Date Extracted: IzzilS
Date Analyzed:
CAS NO.
COMPOUND
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or uq/Kq) (J6~tKC~
h£>
108-95-2	
111-44-4	
95-57-8	
541-73-1	
106-46-7	
100-51-6	
95-50-1	
95-48-7	
108-60-1	
106-44-5	
621-64-7	
67-72-1	
98-95-3	
78-S9-1	
88-75-5	
105-67-	9	
65-85-0	
111-91-1	
120-83-2	
120-82-	1	
91-20-3	
106-47-	8	
87-68-3	
59-50-7	
91-i 7-6	
77-47-4	
S8-06-2	
95-95-4	
91-58-7	
38-74-4	
121-11-	2	
208-96-3	
606-20-2	
-—Phenol
¦bis(2-Chloroethyl)ether_
-2-Chlorophenol_
¦1,3-0ichlorobenzene_
'1,4-Dichlorobenzene~
•Benzyl alcohol^
¦1,2-Dichlorobenzene_
•2-Methylphenol	[
	-4-Methylphenol_
—Hexachloroethane_
—N itrobenz ene	~
—Isophorone
	2-Nitrophenol_
—2,4-0iaethylphenol_
—Benzoic acid	
——2,4-0ichlorophenol_
—1,2,4-Trichlorobenzene_
—Naphthalene^
——4-Chloroaniline
	Hexachlorobutadiene
—4-Chloro-3-methylphenol_
—2-Methylnaphthalene	
—2,4,6-Trichlorophenol_
—2,4,5-Trichlorophenol]
-2-Chloronaphthalene	
—2-Nitroaniline	
—Oimethylphthalate_
—Acenaphthylene_
—	2,6-Oinicrotoluene_
1 HO 1
1













1 1 !
I 1 I






1





1 1
t ,'A T /•> 1
1 \ 1
















i \
I 6 7d> 1
! 3 !
1 
-------
1C
SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE
I
Lab Name:	/= - h *7	Contract: f-'S-eJ-J2V7 | ^
Lab Code:	Case Ho~:.^'U/ZflUhokjiS No.: ________ SDG No.: 	
Lab Sample ID: 7
Lab File ID: "7 L^C It
Date. Received: _~7 /25~/sI
Date Extracted:^
Date Analyzed: s/^i/oI
Matrix: (soil/water) *50!L-
Sample vt/vol:	3 C <£> (g/nL) (r
Level: (low/med) L-dlv
% Moisture: not dec. // *7 dec.	
Extraction: (SepF/Cont/Sonc)
G?C Cleanup: (Y/N) V	pH:	
CAS NO.
COMPOUND
Dilution Factor:
CONCENTRATION "NITS:
(ug/L or uq/Kc' Ut>-lK6~

99-09-2	
—3-N itroaniline
83-32-9	
—Acenaohthene
Sl-28-5	
—2.4-Dinitrochenol
100-02-7	—
—4-Nitrophenol
132-64-9	
—Dibenzofuran
121-14-2	
—2.4-Dinitrotoluene
84-66-2	
—Diethvlohthalate
7005-72-3	
—4-Chloropheny1-phenylether	
86-73-7	
—Fluorene
100-01-6	
—4-Nitroamline
534-52-1	
—4,6-Dinitro-2-methylpnenol
86-30-6	
—H-Hitrosodiphenylamine (1)	
101-55-3	
—4-arcmophenyl-phenylether	
118-74-1	
—Hexachlorobenzene
87-86-5	
—Pentaciiloroohenol
85-01-8 ———Phenanthr ene
120-12-7	
—Anthracene
84-74-2 ————Di-n-buty lphthalate
206-44-0	
—rluoranthene
129-00-0—	Pyrene
85-68-7	
—Butvlbenzylphthalate
91-94-1	
—3.3'-D. -ilorobenzidine 	
56-55-3	
—Benzofa nthracene
218-01-9	
—Chrysene
117-81-7	
—'ois(2-Ethyliiexyl)phthalace __
117-84-0	
—-Di-n-octylphthalate
205-99-2	
—3enzo(b)fluoranthene
207-08-9	
	Senzaric) fluoranthene
50-32-3	
	3enzo(a)Dvrene
193-39-5	
	tndenof1.2.3-cd)ovrene
53-70-3	
	Oibenz 
-------
SEMXVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: Lac-kin &E.J ~~	Contract: (lS		
Lab Code: 	 Case No.	SAS No.: 	 SDG No.:
lREL\
Matrix: (soil/water) *70)L-
Sample wt/vol:	3 0 (q/mL) C-
Level: (lov/med) Z— 0
\ Moisture: not dec. /1 ^ dec.	
Extraction: (SepF/Cont/Sonc) i>Q/\J<£'
GrC Cleanup: (Y/N) V	pH:	
Lab Sample ID: ^ ^}
Lab File ID:
Date Received: ~T J2. /S*f
Date Extracted: 7$/"2 7 jS^t
Date Analyzed: hjlH?
Dilution Factor:
1
CONCENTRATION UNITS: >•
(ug/L or ug/Kg) U£- / K.&-
Mumber TICs found:
CAS NUMBER
i i-i
1.
2."
3
4	•
5."
6."
7 ."
8."
o ,"
10."
11.]
1*5
^ •
13."
14."
15."
16.'
17.'
18.'
19.'
20.'
21.'
22.
23	.
24	.
25	.
26.
27	.
28	.
29.
20.
COMPOUND NAME
5* F 6 6~7 2-
U fS A/O \Va/
ly aJ t< U//I/
U a/ si/a **/ stS	
I	A<3/l rtrSJOfi~s
J	s	
, I c/>2) ** hty/i fl OC Si-r$ be
\U aJ	A a £ si & )oa
.1 U K \*/i/ H-y*> A ae. ,+A to*
.'	HyJ	a laa*kH
1Li±l£L
* *
l£l
EST. CONC. | Q
7 7 A ! V .
*$ 66 1
•ft
1TC. 1
$
/led I

2-6 a i

"/~7  ~2-/a a i

^7^

FORM I SV-TIC
1/37 Sev.

-------
Appendix 5
PESTICIDE CHEMICAL ANALYSES
McFarland, California
El

-------
J.O. 70.27
SEPTEMBER 1989
PBSTICXDB CASE NARRATIVE
FOR MCFARLAHD, CA SAMPLE SET
by
Lockheed Engineering Sciences and Sciences Company
Environmental Programs
Las Vegas, HV 89119
Contract Ho. 68-03-3249
Work Assignment Manager
6. W. Sovocool
Quality Assurance Division
Environmental Monitoring Systems Laboratory
Las Vegas, NV 89114
ENVIRONMENTAL MONITORING SYSTEMS LABORATORY
OFFICE OF RESEARCH AND DEVELOPMENT
U.S. ENVIRONMENTAL PROTECTION AGENCY
LAS VEGAS, NEVADA 89114

-------
METHODS
GENERAL
All glassware was detergent-washed, rinsed with distilled/
deionized water, and rinsed with the appropriate solvent before
use. Quantitative measurements were performed using Class A
glassware.
Pesticides were analyzed by methods prescribed in Exhibit D
of the IFB WA-02 (035/036/081)-Dl protocol. Exhibit D is based
on, but not identical to Method 608, of the Federal Register Vol.
44, No. 233; December 1979.
Sample Extraction
A method blank consisting of 60 grams of sodium sulfate was
extracted with each set of samples. Sample, matrix spike, and
matrix spike duplicate extractions are based on 30 gram aliquots.
The pesticide and BNA fractions were extracted separately via
sonication. The extracts were evaporated to 5 mL, made up to 10
mL in MeC^r and 5 mL of each subjected to GPC clean up.
Pesticide extracts were re-evaporated to 5 mL and solvent-
exchanged to hexane with a final volume of 0.S mL. After the
addition of 0.5 mL of acetone, the extract was passed through 3
grams of neutral alumina (activity Grade III). The column was
further eluted with 10 mL of hexane, and the sample was made up
to a final volume of 10 mL. The Matrix Spike Duplicate (OFOIDS)
extract was lost during the GPC clean up. The sample (OFOl), MS
and MSD results are based on the analysis of pre-GPC extracts.
Sample Analysis
Extracts which were not analyzed directly after extraction
were tightly sealed and stored at 4°C until the analyses were
performed.
Unless prohibited by interferences, the pesticide extracts
were analyzed by GC/ECD with packed-column quantitation and FSCC
confirmation. The instrument parameters were as follows:
1

-------
Quantitation
Instrument:
Column:
Packing:
Support:
Temperature Program:
Inlet Temperature:
Detector Temperature:
Carrier Gas:
Flow Rate:
Injection Volume:
Varian 3400-1
6 foot x 4 mm ID-glass
1.5% SP-2250/ 1.95% SP-2401
Supelcoport 100/120 mesh
190°C l°C/min to 225°C (No hold)
200°C
300°C
Nitrogen
60 mL/min.
2 uL
Confirmation
Instrument:
Column:
Stationary Phase:
Temperature Program:
Inlet Temperature:
Detector Temperature:
Carrier Gas:
Column Head Pressure:
Injection Volume:
Varian 3400-5
30 M x 0.32 mm ID-FSCC
DB-5, 0.25 micron thick
160°C l°C/min. to 230°C.
No final hold time.
200°C
300°C
Helium
10 psi
2 uL splitless
2

-------
RESULTS
GENERAL
The samples were collected by LESC under the direction of
EMSL-LV personnel. NO chain-of-custody paperwork or handling was
requested to be performed. The laboratory personnel did not
receive any written documentation o£ any type.
The extracts were received from the laboratory on August 14,
1989, however, due to the concurrency of other projects
(Quarterly Blind #4 and Pesticide SAS), sample analyses were not
begun until August 19, 1989.
Initial analytical sequences were started on a capillary
column instrument until a packed column unit became available.
Linearity was established and the sample sequence begun. The
first subsequent standard did not meet the CLP-required
specifications, i.e., analyte calibration factors (CFs) RPDs
under 15%. Repeated injections of the standard did not improve
the RPDs and therefore the run was aborted. During the following
few days, difficulties were encountered with the linearity on
both the capillary and packed column instruments. After fresh
evaluation solutions were prepared, new runs were attempted.
Linearity could still not be achieved. After corrective actions
were performed (repacking the packed column, cutting off the
first six inches of the capillary column, and thoroughly
conditioning both instruments), linearity was again achieved.
Meanwhile, arrangements were made to use an alternative packed
column GC. An analysis sequence was started, which met initial
criteria. This sequence was also aborted after the subsequent
standard would not meet the QC requirements.
Analytical sequences were restarted on the packed column anfl
capillary column instruments. The two instruments performed welP
until the second subsequent standard fell outside the QC limits.
Conditioning the columns and repeated hexane injections had no
effect on the problem compounds, most of which were late eluters
(i.e. of higher molecular weight). At this point, it was decide"
to complete the sequences by injecting an ending INDA and INDB,
and using the data obtained so far.
V
One remaining sample needed to be analyzed on both columns.
In addition, the matrix spike duplicate was not analyzed on
the capillary column due to an autosampler malfunction, and
required reanalysis. In order to finish the analysis of all
samples, a new sequence was started on both the capillary and the
3

-------
packed column instruments which had recovered from previous
sample analyses. With permission of the Technical Monitor (G.W.
Sovocool), no PCB or Toxaphene standards were run since none of
these compounds had been detected in the previous samples. The
MSO results for the packed column are included in primary report
package, while the confirmation (capillary) results can be found
in the ancillary data package. Also included in the latter
package are the results for sample R1417. Method blanks were
analyzed on all instruments utilized.
Form I - Organic Analysis Data Sheet
All compound concentrations are reported in ug/Kg. All
compounds were quantitated on the packed column unless
interference prevented doing so.
Only one sample, J212, gave quantitation/confirmation
results greater than the adjusted Contract Required
Quantitation Limits (CRQLs), with a 4,4*-DDE concen-
tration of 1057 ug/Kg. BNA analysis on this sample did
not provide the protocol-required GC/MS confirmation,
however the DDE is shown on the pesticide Form I, for
the user's information. Additional pesticide analytes
below the CRQLs occurred in these samples at the
following frequency:
Compound
4,4'-DDE
4,4'-DDD
4,4'-DDT
a-Chlordane
g-Chlordane
Frequency
(% of samples)
94%
29%
88%
29%
29%
Form.II - Soil Surrogate Percent Recovery Summary
The majority o£ the dibutylchlorendate recoveries are
within the QC limits, however, hydrocarbons,
phthalates, and other matrix interferences present in
the extracts caused high area counts in two of the
samples.
4

-------
Form III - Matrix Spike/Matrix Spike Duplicate Recovery
Nine of the twelve pesticide percent recoveries were
within the QC limits. The two compounds which fell
outside the limits, DDT and Dieldrin, were identified
in the packed column run of the sample which was spiked
(0F01). These compounds were not confirmed on the
capillary run, but the extraneous peaks interfered with
matrix spike compound recovery determinations.
Form IV - Method Blank Summary
The method blanks show no TCL pesticides.
Form VIIID - Pesticide Evaluation Standards Summary
DBC % RSD exceeded the QC limit on the capillary
column, however all quantitations were performed on the
packed column. The RSD for DDT also exceeded 10% on
both columns, and quantitation was performed on the
packed column using a plotted standard curve. The
curve is included in the data package after the
evaluation standard runs (p 215A). On the packed
column, DDT breakdown continually increased as
interferences in the samples contaminated the
chromatographic systems. The DDT breakdown in the
final packed evaluation standard exceeded QC limits.
Of the following five samples, only J212 contained any
DDT or DDT breakdown products greater than the CRQL.
The DDE in this sample was quantitated on the capillary
column.
Form VIIIE - Pesticide Evaluation Standards Summary
All DBC retention times fell within the QC limits for
all four runs.
Form IX - Pesticide/PCB Standards Summary
As has been noted before, the sample matrices caused
severe column degradation which in turn caused many of
the calibration factors to drift out of the QC limit.
The windows for the packed column are based on +/- 1%
5

-------
because there were no retention time standard
deviations available for the repacked columns. Time
constraints precluded running the 72 hour standard
sequence solely to determine RT windows.
Form X - Pesticide/PCB Identification
As mentioned above, the windows for the packed column
are unusually small, which caused some of the compounds
identified to fall outside their windows. In the
judgement of the analysts, all identifications are, in
fact, correct.
"Release of the data contained in this hardcopy summary data
package has been authorized by the Laboratory Manager or his
designee, as verified by the following signature."
J./XV Landers
Senior Scientist
Organic Analysis Section
Environmental Chemistry Dept.
E. A. Steindl
Scientific Supervisor
Organic Analysis Section
Environmental Chemistry Dept
6

-------
"ileNaaa : C:\2700\6CS\nCFS01SF.rM	Data: 8/29/89 10:17 AH Paqa 1 of 1
Start Tiaei 0.00 ain End Tiaa: 70.00 tin Lou Point: 5028 uV Hiqh Point: 16744 uV
Vertical Scale Factor: 0.00 Plot Off sat: 0 aV Plot Scale: 100 aV
Chrcaatogra*

-r-*-
1-4-
u.a
aa
35.01
Tia* (aia)
*.a
a.o
000230

-------
CONCENTRATION OF PESTICIDE STANDARDS IN NG/Ul
MRA
5/10
10/70
25/50
100/200
200/400
230/500
GrBHC
O.OTIS
0.01
0.025
0.1
0.2
0.25
KEFT*JCHLOR
a.QQS
a.ai
0.025
a.i
Q.2
0.25
ALDRfN
0.005
0.01
0.025
0.1
0.2
0.25
HEPEPOX
0.005
0.01
0.025
0J
0.2
0.25
END01
0.005
0.01
0.025
0.1
0.2
0.25
DIELDRIN
Q.Q1
0.02
0.05
0.2
0.4
0.5
DOT
O.OT
0.02
0.05
0.2
0.4
0.5
£ ALDEHYDE
0.01
0.02
0.05
0.2
0.4
0.5
EHDO
0.01
0.02
0.05
0.2
0.4
0.5
METHOXV
Q.Q5
0.1
Q.2S
i.a
2.0
2.5
DBC
o.ot
0.02
0.05
0.2
0.4
0.5
MJXfl
A-SHC
Q.QQ5
a.at
Q.QZ5
a.i
Q.2
a.zs
8-fiHC
0.005
o.ot
0.02S
0.1
0.2
0.25
D-8HC
0.085
0.01
0.025
0.1
0.2
0.25
MDPNN
0.005
0.01
0.025
0.1
0.2
0.25
DOE
Q.01
Q.Q2
Q.Q5
Q.2
a.4
Q.5
ENOKN
0.01
0.02
Q.QS
a.2
0.4
0.5
ODD
0.01
0.02
0.05
0.2
0.4
0.5
E SULFATE
0.01
0.02
0.05
0.2
0.4
D.5
E. KETONE
0.01
a.02
Q.05
a.2
Q.4
a.s
OBC
ff.fff
0.02
0.05
0.2
0.4
u.s
A-CHLOflDANE
0.005
0.31
0.025
0.1
0.2
f!
0.25
G-CHLORDANE
0.005
0.01
0.025
0.1
0.2

-------
SAMPLE TRACKING SHEET
(PESTICIDES/PCBs)
Lot 2.
SAMPLE IDENTIFICATION:
J.0./PROGRAM %
SDG #	 CASE §
IQH:
1.JJ7 //
__ LAB ID.
QA/QC PACK #
Set includes	Reg 9 ID »'s
Sample Type: .Tater SoilJ) Sediment Fish Other	
9S/77
QA Matrix ID ^Ctn^UK. MS ID	MSD ID	RB
Date Received V^c/s-1?		By 7fK	
Date Extracted r7v/c;q		By 	rut - u
Date of Cleanup: Alumina.
GC Analyst 	
GPC g/yj/ift Sulfur.
Date GC Analysis	
SAMPLE PREPARATION
EXTRACTION METHOD: SepF Continuous (^SonicatiorT) other_
Surrogate Lot #
M- 'IP,
Matrix Spike Lot f

Concentration
Concentration
y'j ^' ^
L
EPA Sample #
Region 9 ID
Vol/Grams Extracted
mL Surrogate added
oL Matrix Spike added
GPC Dilution
Final concentrate vol
% Solids / pH
Split latio
(comb, extraction)
1
r-ir-.j
??'"
Tori
j-ur'-

•l^lVr
r>c.ii'S
-if./i „ a —




	:»


















•Wv'iMilf


-------
SAMPLE TRACKING SHEET
(PESTICIDES/PCBS)
A. of jL
SAMPLE IPSNTIFIXATION:
J.
SDG #	 CASE «
IPM IPWTireATlOP:
• 0• /PROGRAM nts.11 JJ\L'/
	 LAB ID.
QA/QC PACK #	
Sat includes q&wr	Reg 9 ID #'s_
Sample Type: Water Soil CsedimenO Fish Other
QA Matrix ID Kinn MS ID 9S//

* irsJ -

.

- >




















1
!
CTMMSFTS ¦

-------
SAMPLE TRACKING SHEET
(PESTICIDES/PCBs)
J. o t jl
SAMPLE IDENTIFICATION:
J.0./PROGRAM
SDG #	
nr.. jn /L*J
LAB ID
CASE «
QA/QC PACK #
Set includes 'K/gV- hs.iwFA Reg 9 ID I's -	
Sample Type: Water <^So£T^ Sediment Fish Other -¦ —
QA Matrix ID ^S/77 MS IOQS;rcMC, MSD ID 9.
-------
SAMPLE TRACKING SHEET
(PESTICIDES/PCBs)

SAMPLE IDENTIFICATION;
J. 0./PROGRAM >7A in	h L „*/
SDG |	
LAB ID
CASE #
QA/QC PACK #
Set includes 9.<;/?g'-1S/9T2& Reg 9 ID #*s_
Sample Type: Water f Soil^ Sediment Fish Other
QA Matrix ID 9S/77 MS ID_2SZSS3il£ MSD ID 9^/^ac rb ID IsnnfLR
Date Received 7/6 c/W		By 		
Date Extracted

Date o£ Cleanup: Alumina,
GC Analyst 	
ay _
gpc *hil/ - 	 Concentration
.viC $
Matrix SpiXe Lot #
Concentration
! C\
EPA Sample #
Raglan 0 ID
Vol/Grams Extracted
mL Surrogate added
mL Matrix Spike added
GPC Dilution
Final concentrate vol
% Solids / pH
Split vatio
(comb, extraction)
>7/«r
A iff.-



/

^n
/











/





/

COMMENTS:

-------
SAMPLE TRACKING SHEET
(PESTICIDES/PCBs)
isticides/
.0./PROGRAM 7/VJ7 /Mc^sL*J SL/v
J, of J.
SAMPLE IDENTIFICATION:
J		
SDG «	 CASE |
<2	 LAB ID_
QA/QC PACK *
Other
Set includes ^nn K/Vtw isuux Reg 9 ID #'s_
Sample Type: Water (^Sail^) Sediment Fish
QA Matrix ID 9S/W MS ID ?C I7SHA MSD ID 9S/g/„/lf RB ID^j^.
Date Rece ived ?/;c/o		By 	j/K	
Date Extracted	2

By
Ctit- W
Date of Cleanup: Alumina v/asrUl GPC^S
GC Analyst 	 Date GC Analysis
Sulfur
avjl_ A.tre-rw 4<=i £Q,^L_) ^	=*<=4-
SAMPLE PREPARATION
EXTRACTION METHOD: SepF
Surrogate Lot # 5T9-7/%
Matrix Spike Lot # ^
Continuous f Sonicatio?
	 Concentration
Concentration
Other
n?.r,A-r- ^ f
J
EPA Sample #
Region 9 ID
Vol/Grams Extracted
mL Surrogate added
mL Matrix Spike added
^ GPC Dilution
Final concentrate vol
% Solids / pH
Split idtio
(comb, extraction)

czrt




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C-C/I-cw^
TOS*/^















4





	
		
		



j.r)~§
j.n*J
2:0 »J






















*TLl
UJiKi- jJoT
I J! J LCtkuJ nsn-&ec
-------
2F
SOIL. PESTICIDE SUBROGATE RECOVERY
Lab Name:, iL-OChjjjidL " c" S C Contract:	~ 3D-H~
Lab Coda: 	 Case Mo.: 	 SAS No.: 	 SDG Mo.
Laval: (low/mad)

EPA
SAMPLE MO.
| SI | OTHER |
|(DBC)#| |
01
f6Lk-1
1 Iff* 1 1
02
P&L ifC-JL
1 HI 1 1
03
OC0\ M.S
1 lot 1 1
04
nC=cf[ OS
1 (6 a. 1 1
05
omi
1 lot 1 1
06

1 IOO 1 1
07

1 9U 1 1
08

1 to* 1 1
09

1 9L 1 1
10
K 4-1 1
I fcr I 1
11

1 93 1 1
12
L 
-------
3F
SOIL PESTICIDE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: LOCKHEED-ESC	Contract: 68-03-3249
Lab Code: Case No.:	SAS No.:	SDG No.:
Matrix Spike • EPA Sample No.:0F01	LOCKHEED SAMPLE NO. 9SI77

SPIKE
| SAMPLE
| MS
MS
QC

ADDED
|CONCENTRATION
(CONCENTRATION
%
LIMITS
COMPOUND
(ug/kg)
| (ug/kg)
1 (ug/kg)
REC #
REC
gamma-BHC (Lindane)-
54
1 o
| 46.5
86
46-127
Hepcachlor	
54
| 0.64
| 50.9
93
35-130
Aldrin	
54
| 0.41
| 48.6
89
34-132
Dieldrin	
136
| 73.1
| 219
107
31-134
Endrin	
136
1 o
| 143
105
42-139
4,4'-DDT	
136
| 36.8
| 228
141 *
23-134

SPIKE
| MSD
MSD
1




ADDED
|CONCENTRATION
«
1
%
QC LIMITS
COMPOUND
(ug/kg)
1 (ug/kg)
REC
#|
RPD #
RPD
| REC
gamma-BHC (Lindane)-
54
| 60.5
112
. .. |
1
26
50
| 46-127
Heptachlor	-
54
| 65.3
120
1
25
31
| 35-130
Aldrin	
54
| 61.3
113
1
23
43
| 34-132
Dieldrin	
136
| 262
139
*1
W-
38
| 31-134
Endrin	
136
| 93.8
69
1
42
45
| 42-139
4,4'-DDT	
136
| 279
178
*|
1
23
50
| 23-134
#	Column co be used Co flag recovery and RPD values with an asterisk
*	Values oucside of QC limits
RPD: O ouc of 6 oucside limits
Spike Recovery:.? ouc of 12. oucside limlcs
COMMENTS:
FORM III PEST-2
OOCOOSL

-------
4C
6 Lk - I
PESTICIDE METHOD BLANK SUMMARY
Contract: U~ OS ~3<2_ ^^
SAS Hp.: 	 SDG Ho.:
Lab Nana: o t£. - CSS
Lab Coda: 	 Casa Ho.:
Lab Sample ID: Q\ S. I % ^
Matrix^soi^/vatar) /O-au I
Data Extracted: -3—
Data Analyzed (1):
Tina Analyzed (1): OOfS
Lab File ID:		
Level: ((loomed) Lo-oJ>
Extraction: (SepF/Cont^Sono) y?rrw c .
Date Analyzed (2):
Time Analyzed (2): 6^-31
Instrument ID (2): \Jo-r 1 ctywO^QQ! Instrument ID (2):	\)gjrig~*r\ 3^QO ~-5"
GC Column ID (1): -2	I Pi<^0 GC Column ID (1):	FSC_C-^7_V^~
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES,	MS AND MSD:

EPA
SAMPLE NO.
| LAB
| SAMPLE ID
01
nPi2*1 ^
1
02
OP?<25f
1 k DS
03
?="(
1
04
HIQ-OS^
1 «7£/jr/
05
m+a?-
1 1x3
06

I -i£fr4-
07
M
1 cl< z^.3.
08

1 r
09
1
1 "IS /**
10

1
11


12


13


14


15


16


17


18


19


20


21


22


23


24


25


26


DATE
ANALYZED 1
DATE
ANALYZED 2
S7.a 


%/£*/&*)

G/**>/&
*JAa/tn


$/2-

Wi/a
COMMENTS!
page J- of
FORM IV PEST
000003
1/87 Rev.

-------
4C
PESTICIDE METHOD BLANK SUMMARY
peuxL
Lab Name':,. UockJk^gcL- F.S, C,
Lab Code: 	 Case No.:
Lab Sample ID:
Matrix:(fsoijv^watarI
Date Extracted: ST- ( ~%°l
Date Analyzed (1): ^"3Q " ^
Tine Analyzed (1):		
Instrument ID (2): \,U Vid.o34£0
GC Column ID (1)	P[CO
Contract: //?8	3
SAS NO.: 	 SDG No.:
Lab File ID:
Level:(tow/med)
Le-uJ
Extraction: (SepF/Cont/gonj) ^ry~
Date Analyzed (2):	jQ5
Time Analyzed (2): 0 3^5*4
Instrument ID (2):
GC Column ID (A) :
vl.
0-V
3l|

THIS METHOD BLANK "APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:
1
1
EPA
SAMPLE NO.
LAB
SAMPLE ID
1
Oil
iyfi4
Q£{°\3
02)

<*s
03 |

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
k£PA SAMPLE NO.
D414
Lab NameI LQCKHEED-ESC
Contracts 68-03-3249
Lab Code«	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
*/. Moistures not dec. 0. 1 dec. 	
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH»
CAS NO.
COMPOUND
SAS No. s ————— SDG No. :
Lab Sample ID: 9S193
Lab File IDs 	
Date Received: 7-25-89
Date Extracted: 8-1-89
Date Analyzed:
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	
319-85-7	
319-86-8	
58-89-9	
76-44-8	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
1 >2*—65—9———
72-54-8	
1031-07-8	
30-29-3	
72-43-5	
53494-70-5	
5103-71-9	
5103-74-2	
8001-35-2	
12674-11-2	
11104-28-2	
11141-16-5	
53469-21-9	
12672-29-6	
11097-69-1	
11096-82-5	
-alpha-BHC		160	U
-beta-BHC		160	U
-del ta-BHC		160	U
-gamma-BHC (Lindane)		160	U
-Heptachlor	—	160	U
-Aldrin		160	U
-Heptachlor epoxide		160	U
-Endosulfan I		160	U
-Dieldr in		320	U
-4,4'-DDE		320	U
-Endrin		320	U
-Endosulfan II		320	U
-4,4'-DDD		320	U
-Endosulfan sulfate		320	U
-4,4'-DDT		320	U
-Methoxychlor		1602	U
-Endrin ketone		320	U
-alpha-Chlordane		160	U
-gamma-Chlordane		160	U
-Toxaphene		3203	U
-Aroc lor-1016—"		1602	U
-Aroc lor-1221		1602	U
-Aroc lor-1232				1602	U
-Aroc lor-1242		1602	U
-Aroc lor-1248		1602	U
-Aroc lor-1254		3203	U
-Aroc lor—1260		3203	U
FORM 1 PEST
1/87 Rev.
cocoes'

-------
Sample Name : D414
Sample Number: 9S193
Operator :
Nelson Analytical 2700 Chromatography System Report Header
4:04 PM
Time
Study
8/31/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
7:03 PM
Raw Data File
Result File
e: \pkd\MCFR038.raw
e:\pkd\MCFR03 8.rst
Instrument File: e:\pkd\pkd.ins
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
'EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Rat Tin Caapoaant	Adjuatad Amount	Raw Amount Paak Araa	Faak Bt MULTIPLIER
(mini Han	UC'K4*	UC[uV-.«c|	[uV]	Ad J/Raw
> n BUTrma	oia»	o.ot eo9T«.a»	ttaa.et	o.o? VC
i n imn«	a. a>	» » a«aaai an	tna*-i in	n n v/C
a m repot	e».ta	aa.n amtf.ee	tfaae.et	a.ay	w*.
w at nmnara	at.aa	iat.n »¦«»«	taiB>a,>o	1 ti VL
n 4* mnni	ta.aa	tuiaiiia	maaei	a.n uc
it.at eat	u».a»	laa.aa i.im	aiaaa.M	a.a? efy
w.ia EiTBAtc	a.aa	i.a» mai na	h*t n»	n ^
23.70 DBC	1*2.13	212.11 2.32a6	60*72.31	0.67
Total Araa - 8733064.00
Tot&i Coetccacr&tloa « 408.1094
Report by Tim Rand, Lockheed-ESC
000003

-------
Chromatoaram
Filename : e:\pfcd\KCFR038.row	Date; 8/31/89 4:04 PH Page 1 of 1
Start Tiae: 0.00 ain End IIm: 47.00 ain Lou Point: -1905427 uV High Point: 1074260 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 av
250.000
166.667
a_>
125.000	
CO
Oj
CkZ
83.133
o
c
o
41.667
-0.000	
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header

Sample Name : D414
Sample Number: 9S193
Operator :
Time
Study
8/31/89 4:30 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D iV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
7:03 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 3 8.raw
e:\pkd\MCFR03 8A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb. smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
»EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Sat Tin Coaponant	Adjuatad Amount Raw Aosuae Paak Araa Paak He MULTIPLIER
[ain]	tfaaa	UC/|^ [uV-».o| [uV] AdJ/Raw
> il 8-8BC
i?a« a onmuin
18.8* BBB
m » m»a
-Mr«
BBB
fl ««
a.aa aaaia.ai naa.at
a.t7
aa.ae
693987.
e?oooi
a.tJ
aa.*i
a
Hl.H
t.83»8 1B1B»B.3B

8.8T
0.67
u.»
i*.3a
33¦ fl* 318893.88 1138I.9T
9. at
¦ 0i67
if


25.70 QIC
tl.73 1838*8i86
U68itt
169.82
233.46
2.82*6 60*72.33
0.67
Total Araa • 6963689.00
Total Coaeantrotloa • 321.5323
Report by Tim Rand, Lockheed-ESC
000003

-------
Chromatogram
FiteUaae : e:\pfcd\NCFR038.rau	Date: 8/31/89 4:30 PN Page 1 of 1	-
Start line: 0.00 ain End liae: 47.00 ain Low Point: -1905427 uV High Point: 1074260 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 av Plot Scale: 250 mV
250.000-
g§ia 3 §
r-
CNI

§
208.333-
166.667-
O-f
125.000—^
crt
o>
CkZ
83.333-
41.667-
O
C
a
c:
O
CJ
0.000-
S CO
I I	I £5 5s 23
I f*! T3! I I I I I*? I iT I Fj
"r~r
£z>
I > T*i i j i i? i i i i i i j r i i i i i i i i | i i i i i i i i i
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator	:
Inter-face #
AutoSampler
Rack/Vial
D414
9S193
S	Channel
None attached
0/0
Time
Study
8/30/89 8:13 AM
MCFARLAND
Data Acquisition Timet 8/30/89 4:37 AM
Delay Time	: 0.00 min.
End Time	: 70.00 min.
Sampling Rata : 1.0 pts/sec
A/D mV Range : 1000
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
Ci\2700\GC5\MCF5036.raw
C:\2700\GC5\MCF5036.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 DG/kg
1
1.00
1.0000
Ar
¦ea Re.iect
: 0.00
Area Threshold
Mult ip1ier
Additive Constant
100
0.67
0.00
Bunch Factors 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400-5'
.2SMM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY IS
PS I
160
200
300
I /MIN TO 230
Total Number o-f Peaks Detected: 93
EXTERNAL STANDARD REPORT
Ret Time
Cmin 3
Component
Name
Adjusted Amount Peak Area Peak Ht Raw Amount
ug\|^ ijftf, CuV-secl CuV3	ug\L
12. 00
.•-> 1 to
G-BHG	
Al nDTKI

a ft?
	770.01	
	r-=rr04	
2*2
	0. 20





i e;7. Q4	
1 01J

ck inn i



585 11
T1 16



1 e:/s



39.22
ENDQ2	
	nn/m ' \	
	1. 70

	0 75.76	
	2. 54-1
l)l>
I
f

-------
40.01 CNDALD	21-. 61	34608.00	1955.25	36.75
461 06 DDT	60 .73 1S1029.11	120S7.73	96r
55. 93 METMOMY	10.28	5668.00 256.6-4	Jr5«r
61.38 DBC	169.44 243194.03 21404.05	252.89


Total Area = 464633.75
Total Concentration = 276.7377
Report by Doherty Bresnahan

-------
FiieNue < C:\2700\GC5\HCF5036.raw	Oate: 8/30/89 8:14 AN Pa?* 1 of 1
Start Tim: 0.00 ain End Tiaa> 70.00 ain Low Point: 3137 uV High Point: 52837 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 100 aV
Chrasatograa
ixgs?;;? e>93
visits »»n»sa
JIJ8-;
%
I "i
D	z
«f	z
Ql
11(7	&3	3J.»	58.33
Tiat (tin)
000012

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Numbers
Operator	:
Inter-face #
AutoSampler
Rack/Vial
0414
9S193
5	Channel
None attached
0/0
Time
Study
8/30/89 9S10 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition
Delay Time	J
End Time	:
Sampling Rate :
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
Noise Threshold
Dilution Factor
Divisor
T imet
0.00
70.00
1.0
8/30/89
min.
min.
pts/sec
4137 AM
C*\2700\GC5\MCF5036.raw
C:\2700\GC5\MCF3036A.rst
C:\2700\GC3\F0E.ins
C:\2700\GC5\EXSTD.pre
Cs\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.67
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument	:VARIAN
Column	:	.23MM
Column Length :	30M
Carrier Gas	:	HE
Flow Rate	:	20CM/SEC
Split Ratio	:
Temperature	:	160
Injection Temp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400 ~ S"
ID .25UMFILM
RTX5
LINEAR VELOCITY 15 F'SI
1/MIN TO 230
Total Number o-f Peaks Detected: 83
EXTERNAL STANDARD REPORT
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin]	Name	ug\j(^	CuV-secJ CuV3	ug\L
10.13 A-8MC	0.07	149.00	13.14	
>12. <14 B-BHC		72.81	
14.64 D DIIC 		717t 19	62.56	
54-r3Q ALDRIN	»r-88		202.02	
29.05 G-CHLDANE	9^-35	1735.00	167.24	
31.02 A CIILDANC	0000 ' u	0-.-65	3272>20 104.00	
t-ro-r
0.32 vj 0
£hr96

-------
34.01 DDC	60.52 302006.00 25102.71	101.96
56.05 ENDRIN	^7.69	10055.66	589.02	11. 47 gf
AO. 81 POO	"-QfiUJs-	SI. 89—34608.00	1855.25	32 ¦ 67 ¦"
—44.60 CNDOOULrATC	2rrtj*	7175.63	5S2'4 29	3. ?gg
51.-28 ENDKETO	15.70	24199.25	1885. 18	23. i
61.38 DBC	21c.25 243194.03 21404.05 321.29
Total Area = 634305.50
Total Concentration = 333.9001
Report by Doherty Bresnahan
ooooi;

-------
FileNaaa : Cs \Z700\GCS\HCFS036.ran	Oatii 8/30/89 ?sil Ml Pap 1 at 1
Start Tiaai 0.00 lin End Tiaat 70.00 tin Lou Point: S1S7 uV High Pointi S2857 uV
Vartical Seal* Factari 0.00 Plat Offttti 0 «V Plat Seal*: 100 aV
Chzoutograi

iimnfih—m—'
us?	&« ma a.a
Til* (lis)
000015

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: LOCKHEED-ESC Contracts 68-03-3249
Lab Code'	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
"/. Moisture: not dec. 2 dec. 	
Extraction: (SepF/Cont/Sanc> SONC
GF'C Cleanup: (Y/N> Y pH:
fciPA SAMPLE NO.
F1204
SAS No. I	SD6 No. s
Lab Sample ID: 9S180
Lab File ID: 	
. Date Received: 7-23-09
Date Extracted: 7-31-89
Date Analyzed:
Dilution Factor:	10
CAS NO.
COMPOUND
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	
319-85-7	
319-86-8	
58-89-9	
76-44-8	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9	
72-54-8	
1031-07-8	
50-29-3	.	
72-43-5	
53494-70-5	
5103-71-9	
5103-74-2	
8001-35-2	
12674-11-2	
11104-28-2	
11141-16-5	
53469-21-9	
12672-29-6	
11097-69-1	
11096-82-5	
-alpha-BHC			
-beta-BHC			
-del ta-BHC		
-g amma-BHC (Lin dane)-
-Heptachlor	
-A1 dr in—	
-Heptachlor epoxide—
-Endosu1 fan I	
-Dialdrin	
-4,4'-DDE	
-Endr in	
-Endosulfan II	
-4, 4' -DDD			
-Endosul-fan sulfate—
-4,4'-DDT	
-Methoxychlor	
-Endrin ketone—		
-alpha-Chlordane	
-gamma-Chlordane	
-Toxaphene	
-Aroclor-1016	
-Aroclor-1221	
-Aroclor-1232	
-Aroclor-1242	
-Aroc1 or-1248	
-Aroclor-1254	
-Aroclor-1260	
163
U
163
U
163
U
163
U
163
U
163
U
163
U
163
U

I 1
/
w
^27
i i
327
u

u
327
u
327
u
327
u
1633
u
327
u
163
u
163
u
3265
u
1633
u
1633
u
1633
u
1633
u
1633
u
3265
u
3265
u
FORM 1 PEST
1/87 Rev.
CCOO ic

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : F1204
Sample Number: 9S180
Operator :
Time
Study
8/30/89 1:51 PM
MCFARLAND
Interface #
Autosampler
Rack/Vial
2	Channel : B A/D iV Range
Varian 8000 without controller
255/255
10000
Data Acquisition	Time: 8/30/89 7:41 AM
Delay Time :	0.00 min.
End Time	:	47.00 min.
Sampling Rate :	1.0 pts/sec
Raw Data File :	e:\pkd\MCFR026.raw
Result File :	e:\pkd\MCFR026.rst
Instrument File:	e:\pkd\pkd.ins
Process File :	e:\pkd\pextstd.prc
Sample File :	e:\pkd\clpa.smp
Sequence File :	e:\pkd\MCFRLND.seq
Inj. Volume
Sample Amount
2 uL
1.0000 uL
Area Reject
: 0.00
EXTERNAL STANDARD REPORT
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
lUe Tlaa
[mini
Adjuatad Amount Raw *nmmf P.*k Aru	at MULTIPLIER
uc/ltfc	0C/K& [uV-.«o| [uV] Adj/JUv
31J9
DD9

t ig «ra renv-
oi aa aiB»t
Hill BittBHIH
u.aa aTBaa-
13.11 DBC
a i ob
.06 H9ga.

1 IB
Dni.n iaan ai
918118.86 1MH.S6
H.O
aaaiaa

i.8t»8 HW«.»
3868*8.86
>i.aa
U.H
li 11.6—38988.
*a»i98
saa.aa
ii>a«< nwa.H
Hi 88
¦ »? 378888l
138.76
201.11
2.68*6 57426.80
a.
-------
Star* !'^e: U.""	tir'			mi	1 •••¦' miii" •'' >« \f " 111911	lis-'4'" m»
MM.. SgM...)MK
cu
CO
cr>
 r-*
J
ji
fr#
-w
n—If'
I	t I
I I
$=> Z
/-n Otd
H
& - g
s s I
1 1 1 n n 1 q
7.83
f I ^1
S
I T"l I I 1 IT ' Fi t" I ' ¦ ' I I ' I
&
rf-
15. 67
T
23 . 50
Time (min)
1 1 1 1 | 1 1 1 1 l 1 1 l 1 | l 1 1 1
31.33	39.17
I I I

-------
Nelson Analytical 2700 chromatography System Report Header
Sample Name : F1204
Sample Number: 9S180
Operator :
Time
Study
8/30/89 2:32 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89 7:41 AM
Delay Time : 0.00 stin.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
Rav Data File
Result File
\pkd\MCFR026.raw
e:\pkd\MCFRQ26A.rst
Instrument File: e:\pkd\pkd.ins
Process File
Sample File
Sequence File
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
Inj. Volume
sample Amount
: 2 uL
: 1.0000 uL
Area Reject
: 0.00
53SSn3SS0BSSSSS
>EXTERNAL STANDARD REPORT1
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Stat Tim	Caapooaas	Ad}u»t«d Amount Raw Amount faak Araa
(mini	Saaa	OS'ltft.	(uV-iae)
Nak ac tm.im.im
[uV] Ad)/Saw
w
||9> » IBS
0 DOB
.0,1(1 » rmfwn»—
19196 081

~«.aa
i»,ii rroniiuttita	
25.n 08C
a.t«
>a.» i»H> .H
> i8t-
li?» 87BH"i„"li		 "W0«t09-
»t.»i 1
at.»


Wi it
t.atm HT91X.U
-M >!¦»!'	
t.tB-
~9*.»a
)999«t.99
et»s»i9t—ny»i 99

H.i)
163.40
2*0.29
2.sa«« i»a.i
»«•-
g'.sr ¦


9 ¦¦¦»»"'

i>.a»	TTM.til 9.98 " \)f~

totai Ana - 177U9M.00
total Csneaatcatlsa ¦ 712. »M2
Report by Tim Rand, Lockheed-ESC

000013

-------

250.000
125.000
83.333	
-0.000	
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : F1204
Sample Number: 9S1Q0
Operator	:
Inter-face # : 5
AutoSampler : None
Rack/Vial : 0/0
Time
Study
8/29/89 1:49 PM
MCFARLAND
Channel
attached
min.
min.
pts/sec
A/D mV Range : 1000
Data Acquisition Timet 8/29/89 12:34 PM
Delay Time : 0.00
End Time	: 70.00
Sampling Rate : 1.0
Raw Data File '•
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
Noise Threshold
Dilution Factor
Divisor
C: \2700\GC3\MCF5024.raw
C:\2700\GC5\MCF5024.rst
C:\2700\GC3\F0E.ins
C:\2700\GCS\EXSTD.pre
C:\2700\GC3\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.68
Additive Constant: 0.00
Bunch Factor!
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN
. 25 MM
30M
HE
20CM/SEC
3400—5"
ID .23UMFILM RTX5
LINEAR VELOCITY 15 PSI
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 104
**********
EXTERNAL STANDARD REPORT
*********
Ret Time
Cmin ]
Component
Name
Adjusted Amount Peak Area
	
CuV-secJ
Peak Ht
CuV3
Raw Amount
ug\L
V
-t-2.39 o one
10.16 HPTCHLR
21.32 ALDRIN
26.09 IICPCPQX
¦30.01 CHDQ1
'¦>. 22
1323.SO
112.12
0. 28
ra3. 00
1» 66	10441. 00
—30.85
631 a 67
-44-»-34	'16863. 44
2994.26
39,74 154110.03	V0426.10
33.07 DIELDniM
000'Uu! J.	05.96 179002.41	13077.24
0: 40
2i 43
- •!>«—
16.68
~0.44- \J
1261 41 if*
A.

-------

END02	

22075i09
—1100156	
	9TSS~



UU 1 J*f i 3 J*

" 1 « "P 1





*•/ * * OUH
Jw • # "r
61.38
DBC
173.52
248222.06
20782.95
258.12
Total Area = 1181495.63
Total Concentration » 576.4711
Report by Doherty Bresnahan


-------
FilaNaaa : C:\2700\6C3MCF5024.rw	Date* 8/29/89 1:30 PH Paga I of I
Start Tim 0.00 ain End Tiaai 70.00 ain U» Point: 5241 uV High Points 83388 uV
Vertical Scala Factor: 0.00 Plot Offset: 0 aV Plot Scalai 100 aV
Cfcroiatograa
1MH
ttaH
k uses	aaaaaassisjssagsstfWfts*;;
* *»8 ctssscxit Ha»**RKi;c:;;;n as* rr aaau n
^iTp#rrrriirtnmninnn!
35,01
TIm (ain)


-------
Nelson Anajytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator	:
Inter-face #
AutoSampler
Rack/Vial
F1204
9S1Q0
5	Channel
None attached
0/0
Time
Study
8/29/09 2:29 PM
MCFARLAND
A/0 mV Range : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
Time<
0.00
70.00
1.0
3/29/89
min.
min.
pts/sec
12:34 PM
C:\2700\GC5\MCF5024.raw
C:\2700\GC5\MCF3024A. rst
C:\2700\GC5\F0E. ins
C:\2700\GC3\EXSTD.pre
C:\2700\GC5\MCFS1B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Re.iect
s 0.00
Area Threshold : 100
Multiplier	: 0.68
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument	:VARIAN
Column	:	.2SMM
Column Length	:	30M
Carrier Gas	:	HE
Flow Rate	:	20CM/SEC
Split Ratio	:
Temperature	:	160
Injection Temp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400 -S"
ID .2SUMFILM
rtx:
LINEAR VELOCITY 15 PSI
1 /MIN TO 230
Total Number of Peaks Detected: 104
EXTERNAL STANDARD REPORT *********
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin]	Name	ug\^£n . •£> CuV-sec3 CuV3	ug\L
10.76
ft DUG	
	0. 12
	023.00
	05.23	
	19 y
12. 3^~
¦D-BMC	
."581
1•wv
ll*.lZ
v • c%J
	^ 50	






20. 99
0 Ci ILDwNC


'Jm / OTl Ate

¦-34.G5
-©ee	
	0000- t	210. 74
720363t00
77854.30	
	309.92 ¦ .

-------

ENDRIN	
25 i Q4
¦33245. QQ
2013.70	
	39.00
44.40
CHDQGULrATC	
	11.39
30460.50
1096*37	
	16.75
Total Area - 2305396.25
Total Concentration =» 759.4067
Report by Doherty Bresnahan

51i04 ENDKETO	SrSi	7914. 00	442.10	7.66	
61.38 DBC	222.98 248222.06 20782.95 327.92


-------
Fildiaaa t C:\2700\GCSMCF5024.pu)	Datai 8/29/89 2:29 FH Pap I of 1
Start Tint 0.00 ain End Tiaai 70.00 ain Lou Points 3241 uV High Point! 83388 uV
Vertical Seals Factori 0.00 Plot QHwts 0 iV Plot Scalai 100 aV
Chxcaatograi
i rssr s=«f;easi6-, i;:as!sc?5sa3 ssr
- *S9 CS 9ICCKI K 3 Aft XI RI9SC3 SC !* Ill III lall III
iusH
».irj
aaH
ii.te-4
I I* •• II IINHiN ««| I llllfl I IMMMMtMM «|| g
WiiwWtf	mm nil
it*	i
m
JL^
I
* lis 3 5
| ?;} 5 ! 9 j$
ff.,. ¦ i iM.-s i 11." i ¦ n | i ¦ 			 i it i
11(7	23,33	35.01	«.tf
Tlat (ain)
58.3

OOOO^S

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHtET
t£PA SAMPLE NO.
H709
Lab Name: LQCKHEED-ESC
Contract: 68-03-3249
Lab Code:	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
7. Moisture' not dec. 0.1 dec. 	
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:	SD6 No.:
Lab Sample ID: 9S188
Lab File ID: 	
Date Received: 7-23-89
Date Extracted: 3-1-89
Date Analyzed: ^
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	
319-85-7	
319-86-8	
58-89-9	
76-44-8	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9—
72-54-8	
1031-07-8	
50-29-3	
72-43-5	
53494-70-5—
5103-71-9	
5103-74-2	
8001-35-2	
12674-11-2—
11104-28-2—
11141-16-5—
53469-21-9—
12672-29-6—
11097-69-1-
11096-82-5—
-alpha-BHC		160	U
-beta-BHC		160	U
-del ta-BHC		160	U
-gamma-BHC (Lindane)		160	U
-Heptachlor		160	U
-Aldrin		160	U
-Heptachlor epoxide		160	U
-Endosul -fan I		160	U
-Dieldrin		320	U
-4,4'-DDE		320	U
-Endrin				320	U
-Endosul -fan II		320	U
-4,4' -DDD		320	U
-Endosul-fan sulfate		320	U
-4,4'-DDT		320	U
-Methoxychlor		1602	U
-Endrin ketone		320	U
-alpha-Ch lor dane		160	U
-gamma-Ch lordane		160	U
-Toxaphene		3203	U
-Aroclor-1016		1602	U
-Aroc lor-1221		1602	U
-Aroc lor-1232		1602	U
-Aroc lor-1242		1602	U
-Aroc lor-1248		1602	U
-Aroc lor-1254		3203	U
-Aroc lor-1260		3203	U
FORM 1 PEST
1/87 Rev.
OOOO <2 ^

-------
Nelson Analytical 2700 Chromatography System Report Header
sssssassssss
Sample Name : H709
Sample Number: 9S188
Operator :
Time
Study
8/30/89 2:46 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
1:55 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume
Sample Amount	:
e:\pkd\MCFR0 3 2.raw
e:\pkd\MCFR0 3 2.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e: \pkd\clpa. snip
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
'EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa	Coapeoant	Adjusted Amount {law Amount Peak Araa Paak Bt MULTIPLIER
[mia]	Naaa	UC/(G|	UC/K£ (uV-»«o) (uV) Ad J/Raw
¦»iM 9 OOB

in at nrnrniM
r»9-
l?isa DBt
'1UI21 UUJJU9-
23.51 DBC
]¦«»
iiii
31inin.ii aan.aa
a.a? »8)a»i98 jmiaa
t i.. aa
ajiiii moii.aa twn.ii
tttiita aiH»«
mm.M nm.ii
>»ia»
II*. 11 8»)>1.U !UU.»»
8i«»
127.as
i.aa
190.8*
2.34a6 334M.93
9iiJ
a.a»

0.67
Ot-
-\l<


Total Araa • 7306937.00
Total Coocaatrattoa ¦ 320.2360
Report by Tim Rand, Lockheed-ESC
000023

-------
Chromatogram
FileNaae : e:\pkd\MCFR032.rau	Oate: B/30/09 2:46 PH Page 1 of 1
Start Tine: 0.00 Bin End IIm: 47.00 ain Lou Point: -IW6777 uV High Point: 1789170 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 raV
u-

-0.000	
7.83	15.67	23.50
Time (min)
31.33
39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : H709
Sample Number: 9S188
Operator :
Time
Study
8/30/89 2:49 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mv Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/39
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
1:55 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 3 2.raw
e:\pkd\MCFR0 3 2A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
A?ea Reject
: 0.00
EXTERNAL STANDARD REPORT
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Rat Tlaa
(min)
Adjusted Amount Raw Amount Peak Ar«« Peak 3t MULTIPLIER
UG'Mk (uV-sac) [uV] Ad J/Raw
i81 9


BBB

at.to sypoggfcTATS
23.57 0BC
0i*0
Oili88
13. 93
ai.u tat.ia
29.06 *99095.08 S6690.68

ia«s
n in antna.ia naaaiaa
aaite
132.77
228.02
2.3*«6 35480.93
a.<7
vt
0.67
a i tT
n is?	\)t-
».6f VK.
0.67
Total Aria ¦ 6913739.00
Toc&X Caocaacracloa ¦ 123.0836
Report by Tim Rand, Lockheed-ESC
0000CJ

-------
		. Chromatogram
FIleNane : e:\pkd\NCFM32.rmi Date: 8/30/89 2:49 PH	Page 1 of 1 ?
Start Tim: 0.00 aln End Tine: 47.00 aln Lou Point: -1446777 uV	High Point: 1789170 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 mV
CLJ
£2
O
cr>
CL>
Ck£
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000
aa "r	\ •*—	o to
s 3 S 9 s 3 :=¦ 3jS
rvi	CM CM CM
CV#	
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : H709
Sample Number: 9S188
Operator	:
Time
Study
8/30/89 7:36 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range J 1000
Data Acquisition Timet 8/29/89 9:11 PM
Delay Time
End Time
Sampling Rate
Raw Data File :
Result File :
Instrument File'
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC3\MCF5030.raw
C:\2700\GC3\MCF5030.rst
C:\2700\GC5\FQE. ins
C:\2700\GC5\EXSTD.pre
C:\2700\GCS\MCF51A.smp
C:\2700\GC5\MCF54A. seq
2 uL
1.0000 UG/kg
Area Reject
: 0.00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold s 100
Multiplier	: 0.67
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument	:VARIAN
Column	:	.25MM
Column Length	:	30M
Carrier Gas	:	HE
Flow Rate	:	20CM/SEC
Split Ratio	:
Temperature	:	160
Injection Temp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400 - 3
ID .2SUMFILM
RTX5
LINEAR VELOCITY IS PSI
1/MIN TO 230
Total Number o-f Peaks Detected: 94
EXTERNAL STANDARD REP0FTT
*********
Ret Time
CminD
Component
Name
Adjusted Amount Peak Area Peak Ht Raw Amount
ug	CuV-secD 1uV]	uq\L
13.56 SrtBMC
-18.26 HPTCHLR
nnjnirr-
*h. 71 HFPFPflV
-1.88	11523i-se	576i 25
-O-rSe	©71-. 00-	6?t94-
o.ss isat.tfc toa.iq
0.37	S785. 00
US.63
SO.09 EMDQ1	
55.94 0IELPRIM
¦IS. 65	61510.00
4556u 73
2.Q1-
0. 45
0. 37-
0. 85
. j-j
74.27
49.76 10S635.11
8295. '10
oooo.;

-------
TB.23
a 1 -***
EMP03	
CTMr\/\i r\
	3. 03
—10339. 0'> ¦
	061.70	


PT>T

11 ni4!-" 11
IB
B1


4 A ^



61.37
DBC
202.66
290880.00
26941.24
302.48
Total Area = 647012.44
Total Concentration - 336.6638
-cos
Report by Doherty Bresnahan
0000:3

-------
FU«*aaa : C:\2700\GC3\KFS030.rw	Data: 8/30/89 7:36 AM Paga 1 of 1
Start Tiati 0.00 ain End Tiaa» 70.00 ain Low Point: 3230 nV High Point: 45571 uV
Vartical Scala Factor: 0.00 Plat Offset: 0 aV Plot Scala: 100 aV
Chrcaatogra*
1IMH
asH
MH
m-.
sua-:
5 nt.sa* sass? K3 «s.a5sa*ns.s*»flcsxs	* s
* *;s:s ssscx «c; rao*HR*«5s«saMr Miaaag i t

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : H709
Sample Numbers 9S188
Operator	:
Inter-face # : 5
AutoSampler : None
Rack/Vial : 0/0
Channel
attached
Time
Study
A/D mV Rang*
8/30/89 0156 AM
MCFARLAND
1000
Data Acquisition Timet 3/29/39 9«11 PM
Delay Time	:
End Time	:
Sampling Rate :
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume :
Sample Amount :
Noise Threshold:
Dilution Factor:
Divisor	:
0.00
70.00
1.0
mxn.
min.
pts/sec
C:\2700\GC5\MCF5030. raw
C:\2700\GC3\MCF5030A.rst
C:\2700\GC3\F0E.ins
C:\2700\GC3\EXSTD.pre
C:\2700\GCS\MCF31B.smp
C:\2700\GCS\MCF54B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.67
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
3400
ID .2SUMFILM RTXI
VARIAN
. 2SMM
30M
HE
20CM/SEC LINEAR VELOCITY
15 PSI
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected* 94
Ret Timi
Cmin]
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
	CuV-sec]
Peak Ht
CuV]
Raw Amount
ug\L
$4
40.40 A--BHC
i 1 AO p-pur
(4,
P-BHC
H.59 nLDRIM
29.09 5-CHLDANE
;i.OO A-CIILDAME
4-800.4;

13-
:938.o:
¦tag. 4a
t. 91
0.58
3026.50
¦186.42
-Or-8-7
0.26	1506.66
140.39
i 09 130203.'10	10011.23
- XLUTT'
21 ¦ 80 110112.55
0.39
T.8-. 64 ^
0526.06
32.63 ^
0000^:;

-------
34.61
-BBE	
	64.05
2Q307Q* 56
23970,99	
	9S-. 60






4U»
A A **0
e?Kmr*ei n catc

KJ'Jt ^ U •
-r l.
14 A A
' w.i r>-r
rKini/CTn
** 61
5559 a**
^Q9 i

61.37
DBC
137.46
290880.00
26941.24
384.27
Total Area = 944693.6?
Total Concentration = 443.6092
Report by Doherty Bresnahan
OOOOoS

-------
FilaNaaa : C:\27M\GCS\fCF3030.ru	Data» 8/30/89 8»37 AH Pip 1 oi 1
Start Tiaat 0.00 tin End Tiaai 70.00 ain Low Point! 3230 uV High Points 45371 uV
Vertical Scale Factor: 0.00 Plot Offwt: 0 aV Plot Seals: 100 aV
Chzoaatograa
UUH
tua-4
JUB-j
!$.KH
ia
•	nc.sa* ssssss ss ss.a;sa*8*^3^sir;*5 *89943 * *
*	*-SSS 99KBZ IK ft 9M ftX RR99 S7SSS 8BB N MRlBB I I
iimrimr
It I
^u.

it	i i	i	»
u . 1
ILlLi I
11(7	23.33	35.01	5133
Tix* (lis)
>
00007/

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHtET
tPA SAMPLE NO.
11205
Lab Names LOCKHEED-ESC
Contract: 68-03-3249
Lab Codes	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vois 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 0 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH»
CAS NO.
COMPOUND
SAS No.:	SDG No. :
Lab Sample ID:	9S181
Lab File ID:		
Date Received:	7-25-89
		Date Extracted: 7-31-89
SONC	Date Analyzed:
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	a lpha-BHC	
160
U
319-85-7	beta-BHC	
160
u
319-86-8	del ta-BHC	
160
u
58-89-9	gamma-BHC (Lindane)	
160
'J
76-44-8	Hep tach 1 or	
160
u
309-00-2	Aldr in	
160
u
1024-57-3	Hep tach lor epoxide	
160
u
959-98-8	—Endosul fan I	
160
u
60-57-1	D i e 1 dr i n —	
320
u
72-55-9	4, 4'-DDE	
320
u
72-20-8	Endrin	
320
u
33213-65-9	Endosul fan II	
320
u
72-54-8	4, 4' -DDD	
320
u
1031-07-8	Endosul fan sulfate	
320
IJ
50-29-3	4, 4' -DDT	
320
'J
72-43-5	Methoxychlor	
1600
u
53494-70-5	Endrin ketone	
320
u
5103-71 -9	a 1 pha-Ch 1 or dane	
160
u
5103-74-2	gamma-Ch 1 or dane	
160
u
8001 -35-2————Toxaphene	
3200
u
12674-11 -2	Ar oc 1 or -1016	
1600
u
11104-28-2	Aroclor —1221	
1600
u
11141-16-5	Ar oc 1 or -1232			
1600
u
53469-21 -9	Ar oc 1 or-1242	
1600
u
12672-29-6	Aroc 1 or-1248	
1600
u
11097-69-1	Aroc lor-1254	
3200
u
11096-82-5	Aroc lor-1260	
3200
u
FORM 1 PEST	1/87 Rev.
000C3&

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number:
Operator :
Interface #
AutoSampler
Rack/Vial
11205
9S181
Time
Study
8/30/89 1:53 PM
MCFARLAND
2	Channel : B A/D raV Range
Varlan 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
8:33 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR027.raw
e:\pkd\MCFR027.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
~EXTERNAL STANDARD REPORT*
Instrument 10: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa	Cn«p
-------
FileNaae : e:\pfcd\NCFR027.raM	Date: 0/10/89 t;54 PH Page 1 of 1
Start Ii*e: 0.00 ain End ?!¦>: 47.00 ain Low Point: -1869957 uV High Point: 999100 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 mV
250.000
208.333
166.667
cr
o
<—i
41.667
0.000
I
7

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface #
AutoSampler
Rack/Vial
11205
9S181
Time
Study
8/30/89 2:34
MCFARLAND
PM
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
1GQG0
Data Acquisition Time: 8/30/89
Delay Time : 0.00 ain.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
8:33 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR027.raw
e:\pkd\MCFR027A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.prc
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
S33S38S
*****EXTERNAL STANDARD REPORT*****
!¦¦¦	ir 11			¦		iMidriii
Instrument ID: varian 3400-1	GC Column ID: 2250/2401
Tta
[mis)
8aaa
MJuatatf Amount Raw Atoou&e P«ak Aru P»mk as HOITITtZEB
tuV-t«e] (uVl Adj/Ra*



























•*h
iM lil
laa
p**—
	-Wi



	»!»¦
BBB
Uill B1IM8WUMB
23.36 BSC
»i»8	
lt.il'
—3J18.89
maiu.uu
	e»i0»
178.03
81,83 IWM.BB
•nm.jf
mm. a*"
233.7?
Z.Slaft 64896.32
-trrr
-5T9T-
0.67
i
-------
„ , ,	Chromatogram
FileMaas : e:\pkd\HCFR027.rau Date: 8/30/89 2:34 PH	Page 1 of 1
Start Tine: 0.00 ain End Ttae: 47.00 atn Low Point: -1869957 uV	High Point: 999100 uV
Vertical Scale Factor: 0.00 Plot Offaet: 0 MV Plot Scale: 2S0 nV
CLJ
CO

250.000-
208.333-
166.667-
12S.0O0-
83.333-
41.667-
-0.000-
O
o
o
o
ro
uu
3

QC3 U~>
£ S
• • • •
• • • •
YrrtYtfi"
III	I I I
hi =
n co
I	I
I
c . to r— crv	. .	_ 	
sags gg g g
cr»
PI
& g
Ln
S


(C
«£
i i"*i *Fi i i i i i*? i i i i i i i i T*i i | i i'? i i i i i i [ i i i i i i i i i | i i i i i i i i
I 311

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : 11205
Sample Number: 9S181
Operator	:
Time
Study
8/29/99 3:09 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time: 8/29/89 1:40 PM
Delay Time : 0.00 min.
End Time	: 70.00 min.
Sampling Rate '¦ 1.0 pts/sec
Raw Data File :
Result File :
Instrument File>
Process File
Sample File :
Sequence File :
Inj. Volume :
Sample Amount
Noise Threshold:
Dilution Factor:
Divisor	:
C:\2700\GC3\MCF3023.raw
C:\2700\GCS\MCF502SA.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF31A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.67
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400-ff
.23MM ID .23UMFILM RTXS
30M
HE
20CM/SEC LINEAR VELOCITY
13 PSI
160
200
300
1/MIN TQ 230
otal Number o-f Peaks Detected: 79
EXTERNAL STANDARD REPORT
*********
Ret Time
[min ]
Component
Name
Adjusted Amount Peak Area
ug

<\0
CuV-sec2
Peak Ht
CuV]
Raw Amount
ug\L
4
»39
lQi 93
0 DUG
•0. 11
01 21
Oi 77
069.00
06.75
¦<*T
«-#¦
HPTCIILR
11.26 ALDHIN
-r±rw
¦C6. Z2 HEPCP0X
'0.16 END01
¦33.07 DICLDRIN
—611.00
49141 00
36.03
302.30
0.31
1203.GO
15.85	62397.50
000043
-H*-
6732.00
-mi
415.30

-tr*5—Lr
—79.98	
3281.15	*?iTi ¦ .« ^ -
23.66
4. 73



-------
5Q. 16
CHDQ2	
	1. 32
4QS6»Q0
	311 * 20	
	2. 12












• U «L
61.38
DBC
w • / U
200.14
X Q7 •
287263.00
Jut • 4J»
23934.51
a • ww
298.71
Total Area = 440387.19
Total Concentration 53 261.6631
sport by Doherty Bresnahan
000044

-------
FileHaaa : C:\2700\eCS\ICF502S.ru	Oatai 8/29/8*7 3:10 PR Page 1 o* I
Start TiaX 0.00 ain End Tiaai 70.00 ain Low Points 5247 uV High Point! 56544 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Cfcraaatograa
* t9 S3 S SS38 ; * *3 9 8
; 58 55 fl	lilill
- *95 9 SRsRCXfc JU«* Hli**
m
1
ft
i$«-
110	23.33	35.01	«.»	9.33
Tia* (ain)
00004s"

-------
Nelson Analytical 2700 Chromatography System Report Header
¦ VMaaMKBaiiaiWataxaaKaiwaMaxiaa	I	—	£			 '
Sample Name ; I1203
Sample Number: 9S181
Operator :
T ime
Study
8/29/89 3:05 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range i 1000
Data Acquisition
Delay Time	:
End Time	:
Sampling Rate '•
Raw Data File s
Result File :
Instrument Files
Process File s
Sample File 5
Sequence File '
Inj. Volume :
Sample Amount i
Tim#i
0.00
70.00
1.0
8/29/89
min.
fli i n •
pts/sec
1s 48 PM
C:\2700\GC5\MCF5023.raw
Cs\2700\GC5\MCF5025. rst
C:\2700\QC5\F0E.ins
C:\27Q0\GC5\EXSTD.pre
C:\2700\GC3\MCF51B.smp
Cs\2700\GC5\MCF54B.seq
2 uL
1.0000 U6/kg
Area Reject
0.00
Noise Thresholds 1
Dilution Factor! 1.00
Divisor	: 1.0000
Area Threshold	100
Multiplier	s 0.67
Additive Constants 0.00
Bunch Factors 1
3400
ID
Instrument Conditions!
Capillary GC -
Instrument	sVARIAN
Column	s	.23MM
Column Length s	30M
Carrier Gas	:	HE
Flow Rate	s	20CM/SEC
Split Ratio	s	¦
Temperature	:	160 1/MIN TO
Injection Temp.!	200
Detector 1	:	300
Detector 2	:
Notes	*
- 5*
J3UMFILM
RTX5
LINEAR VELOCITY 15 PSI
Total Number of Peaks Detected! 79
xtitttnn
EXTERNAL STANDARD REPORT

Ret Time
CminJ
Component
Name
Adjusted Amount Peak Area Peak Ht Raw Amount
CuV-sec3 CuV3	ug\L
10.76 A D1IC
rWr
403.00
60v 53"
0-y 09-
i -r-r


	>>. 5?	
	86Ch
-------
¦-5A.75 EMDRIM	S^SS	3697.00	175. 49	1.23 ¦¦ lA'"'
40.39
486	
	IS. 12
25905.00
IBIS.01	
	22,57
• -51.55-
LNUUwULI l! 1 L
ENDKCT0	
0.25
	301100
/7
j5 • jQ
¦ J • 38
0,57
IA
4>
61.38 DBC	254.26 297263.00 23934.51	379.49
Total Area » 1007720.56
Total Concantration «¦ 425.7055
Report by Doherty Breanahan
000047

-------
FilcNtaa t C:\2700\GC3VCJT023.rw	Oatt: 8/29/89 3:06 PN Pa$» 1 of 1
Start Tiaa» 0.00 ain End Tint 70.00 ain Low Point! 32*7 uV High Points 36344 uV
Vertical Scaia Factor« 0.00 Plot Offset! 0 aV Plot Scalai 100 aV
Chzoaatograi
:s;> ssss*«9 sac ?sax z, *m 9 9
IS BBSS Mafift HUM		
9 a i ami
I
m
m
I
w
firnrri
11(7	23.33	35.®	<4.0	St.33
Tia* (ain)
000048

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J212
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Code:	 Case No. s
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
7. Moisture: not dec. 0 dec. 	
Extraction: 
-------
Nelson Analytical 2700 Chromatography System Report Header

Sample Name : J212
Sample Number: 9S191
Operator :
Time
Study
8/31/89 3:59 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
5:20 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR03 6.raw
e:\pkd\MCFR0 3 6.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
0.00
*EXTERNAL STANDARD REPORT"
Instrument ID: Varian 3400-1	GC column ID: 2250/2401
Rat Tlaa
(mini
Adjuatad Amine Raw Aaount P«ak Araa Paak Be HOLTXTLm
0C lf(&	[uV-sae] [u»] Ad]/Raw
MMBBO-

OHMRIH
ht at nmaa
-W-r
0B*
10 to niBAfcB
23.10 DBC
u. >«
ttnaa.aa—iwi.83
taniH
oii»e
¦ >8ia aafiB.iii
.00a? O.tiat

T«-
oo»a t«aiee.i«
t.tit
n.so aiatoo.
t.i
-------
Chromatogram
FileNane : e:\pkd\MCFR036.rau	Date: 8/31/89 4:00 PH Page 1 of 1
Start Tine: 0.00 atn End Tiaa: 47.00 afn Low Point: -2145987 uV High Point: 1885510 uV
Vertical Scale factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 nV
250.000
208.333
166.667
12S.000
-0.000
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : J212
Sample Number: 9S191
Operator :
Time
study
8/31/89 4 5 26 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/2S5
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
5:20 PM
Rav Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume
Sample Amount
e:\pkd\MCFR03 6.raw
e:\pkd\MCFR036A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
: 2 uL
: 1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rae fUm
taial
Adjusted janit Raw Amount P««k Azaa
UG/yfx	UO/f ^ (uV-«ae»
I>Mk Ht HOLTITLia
(uV) Ad]/Saw
».i an »-»8c
ti rwimr

'*!>	il
&*** mm

1J.J1 ABB
Miii mctmnn
aii»a 8
rggrria-

8 78
" "	-- •«" I'
.ia *x.
a		
u at
ta.ta aiBBBa.aa nmi
¦**-
sn,n inati.n aixnna*	

-V*-
¦\j<-
—§»¦»»'
13**.09
m.w
a«.w
o»ua
2008.11
agi'iaa	
ioTsaaa
*.08a?
aa.a« iiaiaai
3.*3ai
i»oiae.n
soatiM
9. 6?
O.il
-#*W-
O.tt


I
IM&
Total Araa - 3033*721.00
Taut Coma Titration « 1770.0*07
Report by Tim Rand, Lockheed-ESC
000052

-------
Chromatogram
FileNane : e:\pkd\HCFR036.rau	Date: 0/J1/09 4:26 PM Page 1 of 1
Start line: 0.00 min End lias: 47.00 sin Lou Point: -2145987 uV High Point: 1885510 itl
Vertical Scale factor: 0.00 Plot Offset: 0 MV Plot Scale: 250 cnV
250.000
208.333
166.667

-------
Nelson ^alyHcalJ700 Chromatography System Report Header
Sample Name : J212
Sample Numbers 9S191
Operator	:
Time
Study
8/30/89 3:07 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount :
Noise Threshold:
Dilution Factor:
Divisor	:
Tit
0.
me:
00
70.00
1.0
8/30/89
mih.
min.
pts/sec
2:09 AM
C:\2700\GC5\MCF5034. raw
C:\2700\GC3\MCF3034.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GCS\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject
0.00
Area Threshold : 100
Mu11 i p1i er	: 0.67
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY II
PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 113
**********
EXTERNAL STANDARD REPORT
*********
Ret Time
[min D
Component
Name
Adjusted Amount Peak Area Peak Ht Raw Amount
ug\|^	CuV-sec3 CuV3
VS. AO
1 « a er
15-BHC	
udttui e»

0. 37
	1597.7;
	1 flfl.SS	















T* 1 T
c-Kinrv-j

'J 1 U J
A
1rt7Q^fl OA
7A IT ^


DICLDHIM	

	54. 10
11H905.00
9227.22	
	00.01 B:
0000S4

-------
30. 15 CMDOO 3136 11467 4 00 790h6S	5.01
'11.14 CNDALD	2t&2	3962.00 270.40	4.20	
45.99 DDT	36.06—964604 56	703B.Q3	55.01 **
55.90 METMOXV <1.03	3514.00	101. ZO	4.08 l/C.
61.33 DBC 218.02 312928.56 27293.15	325.40
Total Area = 646161.69
Total Concentration =» 348.1918
Report by Doherty Bresnahan
000055

-------
FiltNaw : C:\2700\GC5\MCF3034.rw	Datai 8/30/89 8:08 AH Pag* 1 ai 1
Start Tint 0.00 tin End Tint 70.00 ain Lom Point: 5254 uV High Pointi 374964 uV
Vertical Seal* Factor) 0.00 Plot Offttti 0 aV Plot Seals! 100 aV
Chxoutograa
UWH
ttm-j
JUB-i
5WH
1MB-!
ft g*iriije«*S5JSS9 S?3*.= 38S; *3	ftWBS R 5 6 88 ss
- '•"•SS58SS3« BCBIICRRR RR«#;55S55 RMS** 1} II 61
• » «•
¦ MMIII •IMfIMN
•	MMtl
^Tiriiinriiiini^iiri'iiiiViiTfrfll^fl Annn IpiniflA^r
i	I	i
I h,I it, II
11(7 as s.»
Tlx* (aia)


000056

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : J212
Sample Number: 9S191
Operator	:
Tima
Study
8/30/89 9:04 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5
None
0/0
Channe
attached
A/D mV Range « 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount :
Noise Threshold:
Dilution Factor:
Divisor	:
Time: 8/30/89 2:09 AM
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GCS\MCF3034.raw
C:\2700\GC5\MCF5034A.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.prc
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.67
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument	:VARIAN
Column	:	.25MM
Column Length	:	30M
Carrier Gas	:	HE
Flow Rate	:	20CM/SEC
Split Ratio	:
Temperature	'•	160
Injection Tamp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400-5"
ID .23UMFILM RTX5
LINEAR VELOCITY 15 PSI
1/MIN TO 230
Total Number o-f Peaks Detected! 113
"•••*•"* EXTERNALSTANDARD REPORT***"*****
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
Cm in]	Name	ug\fcj*	CuV-sec] CuV]	'-igNjCjJ
10.31
VI QQ
A-BHC	
o—ciur


	1098.00—
no
	91.23	
¦^7 n?
	»r-94
—oi in





4 « rt

^ 4 tr a
a i nntki

/-\~T










30.70
A CIILDANC	
	000057
	17.61
09216,73
• JU
6017.31	
	26.28

-------
34.54 ODE
1037.:
4.68a6 369625.31
1578.11

EMPBIM	

1S17B.84
	784.45	



- 1 o
I 'J 1 4^ I Uv
"fwv / ii^UU
-o-O ^ 1
Jl'/« 1U
/i -rer
51.21
& 1 • 3w
ENDKETO
OBC
11.57
276.98
17843.44
312928.56
1009.96
27295.15
17. 27
413.40

Total Area - 5758359.00
Total Concentration = 1736.4827
Report by Ooherty Brssnahan
000058

-------
FileNut : C:\2700\6C3\HCF5034.rM	Dat«: 8/30/89 9:05 AH Paw 1 of 1
'tart Titti 0.00 tin End Tiat: 70.00 ain Law Point: 5224 uV High Point: 374964 aV
ertical Scale Factor: 0.00 Plot Offset: 0 «V Plot Scale: 100 aV
Chroiatogra*
ft S!S)eR)t«?S);«IS5S5*riS2?«I6«aRl;«;3«6Sf>5ft S3
- *«'i«1s»ssse5 Z RGRRSCBRR Hft ¦5:5:555 T	
8RH S I P 8 a iB 32

11
n
5
a
n
«
!{»•
"f-TW iw nriiimnWirar'TTiri
si is
33.01
11(7
Tiw (ain)
000059

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
tPA SAMPLE NO.
K411
Lab Names LOCKHEED-ESC
Contract: 68-03-3249
Lab Codes 	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/voli 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 0.2 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No. • 		SDCb No. :
Lab Sample ID: 9S190
Lab File ID: 	
Date Received: 7-25-89
		Date Extracted: 3-1-S9
SONC	Date Analysed:
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	0
319-84-6	alpha-tfHC	
160
U
319-35-7	beta-BHC	
160
U
319-86-3	del ta-BHC	
160
LI
58-39-9	gamma-BHC 'Lindane)	
160
; i
76-44-8	Heptach lor	
160
u
309-00-2	A1 dr in	
160
u
1024-57-3	Heptach lor epo:: i de—		
160
u
959-98-8	Endosulfan I		
160
u
60-57-1	Die 1 dr in		
321
u
72-55-9	4, 4'-DDE	
321
u
72-20-8	Endr in	
321
u
33213-65-9	Endosul-fan II	
321
u
72-54-8	4, 4'-DDD	
321
IJ
1031-07-8	Endosul tan su.l -fate	
321
u
50-29-3	4. 4' -DDT	
321
u
72-43-5	Methoxych lor	
1603
1
u
1 1
5103-71-9	-a lpha-Ch lor dane	
160
IJ
IJ
5103-74-2	gamma-Ch 1 or dane	
160
!J
S001-35-2	Toxaphene	
3206
u
12674-11-2	Aroc lor.-1016	
1603
u
11104-28-2	Aroc 1 or-1221	
1603
u
11141-16-5	Aroclor-1232	
1603
u
53469-21-9	Aroc lor-1242	
1603
IJ
12672-29—6	Aroc lor-1248	
1603
IJ
11 C°7—69— 1	Aroc 1 or-1254	
3206
IJ
110'6-82-5—		Aroclor-1260	
3206
u
FORM 1 PEST	1/37 Rev.
CCC06 0

-------
Nelson Analytical 2700 Chromatography System Report Header
S333SS:
Sample Nana : K411
Sample Number: 9S190
Operator	:
Time
Study
8/31/89 3:57 PM
MCFARIAND
Interface #
AutoSampler
Rack/Vial
2	Channel :
Varian 8000 without
255/255
B A/D mV Range : 10000
controller
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
3:37 PM
Raw Data File
Result File :
Instrument File:
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount
e:\pkd\MCFR034.raw
e:\pkd\MCFR034.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
~~~~•EXTERNAL STANDARD REPORT^^*
Instrument IDs Varian 3400-1
GC Column ID: 2250/2401

Rat Tim
[min]
Hftoa
Adjuatad Aaount Raw Amount
05 !%£ ue/i
P«ak Art*
[uV-».c]
Faak Ht
tuV)
KULTIPLIEH
Ad J/Raw















BBPB1
¦	 ¦ r j,Q3




23.44 DSC
81.50	
113.IS
a».ti tTstea.M—otaa.i*
189.18
2.23*6 51393.38
0.61	
0.8?
Vic
rfk-
_y
Total Art* - 4188671.23
Total Concentration - 183.8933
Report by Tim Rand, Lockheed-ESC
000061

-------
stf-
"'^¦1 : MhI ""bB

Cxi
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
m	U> -r
—. <=J ^
cn	S rvi
iii 'i r ¦ i
-~J-V-rrAr--~r
¦	• ¦ ' i ' '	a	¦¦
<6
CJ
;3
c?
c>
o
i	i i
i i
7.83
39. 17
23 . 50
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : K411
Sample Number: 9S190
operator :
Time
Study
8/31/89 4:23 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mv Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time:	8/30/89
Delay Time : 0.00	min.
End Time : 47.00 min.
Sampling Rate : 1.0	pts/sec
3:37 PM
Rav Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR034.raw
e:\pkd\MCFR03 4B.rst
e:\pkd\pkd. ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 UL
1.0000 UL
Area Reject
0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Ric Tlaa	Covenant	Adjuatad Mount Rav Amount Paak Araa P«*k fl« MULTIPLIES
[mini	Haas	{«»-••«1 iu«] MJ/Slav




















i










25.64
0BC
133.
.*3
202.
,1*
2.23*6
21393.58
0.6?

v*»
Total Atmm - 41260*1.7S
Total Concentration « 207.SIM
Report by Tim Rand, Lockheed-ESC
000063

-------
Chromatoqram
Filename : e:\pkd\HCFROM.rau	D..10: 8/31/89 4:24 PM Page 1 of 1
Start Tine: 0.00 ain End Tiae: 47.00 ain Low Point: -2038747 uV High Point: 1117300 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 nv
a_>
cV>
cr
cr>
ex:
250.000-
208.333-
166.667-
125.000-
83.333-
O
o
o
Qll.667-
a
•0.000-

e
•%r

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
K4U
9S190
Time
Study
3/30/89 8:01 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range • 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Time J
0.00
70. 00
1.0
8/29/89
min.
min.
pts/sec
11:40 PM
C:\2700\GC5\MCF5032.raw
C:\2700\GC3\MCF5032.rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.prc
C:\2700\GC5\MCF51A.smp
Cs\2700\GC5\MCF54A.seq
Ini. Volume
Sample Amount
2 uL
1.0000 UG/ka
Area Reject
: 0. 00
Noise Threshold: 1
Dilution Factor: 1.00
Divisor	: 1.0000
Area Threshold
Mult ip1ier
Additive Constant
100
0. 67
0. 00
Bunch Factor-
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
3pIi t Rat i o
Temperature
In.iection Temp.
Detector- 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 32
********** EXTERNAL STANDARD REPORT *********
Peak Ht Raw Amount
r i,i; t	11 a v i
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin]	Name	ug	CuV-sec2 CuV]	ug\L
21. 23 flLDRIN	^	204. 00	32. 19	0. 0~ '
30.13 END01		e-rw	1-285.00	-85". 99	 	0. 49 ¦
u~.S-1 PIELDBIN	UrZZ	2916. 44	188.05	2. 05
35. 15 END02	0. SO	1714. 00	90.63	*
40.74 CNDALD	-4ri-l	5779. 00	310. 66	tr
• 16. 02 DDT	12. 44	29191. SO 2627.54	19.57
2.US ^ -J
0. 75
trr*€ U0-*
000065

-------
—~ i ii>J 11931 00 ZS8« 99	11» 'T'S
149.38 214701.50 10853.04 223.26
Total Area = 260064.44
Total Concentration = 175.9857
55j 04 WCTIIOXV
61.40 DBC
Report by Doherty Bresnahan
000066

-------
FilcNm : C:\2700\GCS\NCF5032.rM	Date» 8/30/89 8:02 AH Page 1 of 1
Start Tioai 0.00 ain End Tiasi 70.00 ain Low Point! 3238 uV High Pointi 42669 uV
Vertical Scale Factor: 0.00 Plot Offsets 0 «V Plot Scale: 100 aV
ChrosatograB
R
d

6 5? 5 3
S Z 9 KG
TCSSS! i. a) i s it ^ s
kiurx mi? :s ? fln&aa a
%
Jur|
JI
4 II
Ji!
in
3-4-v-r-
M Ml*	1 *
ii II li	it
I
¦nmmi'i nrrn—i:n n n mi M—rr
'l I • ¦ * - I a 8	I
1 fii5 1 11 § I
, i 11" ¦ * i " i i r. i 9 i i i r. ¦ i ,B	?¦
1U7
23.33
35.00
TiM (tin)
14.67
58.33

Q000«7

-------
Nelson Analytical 2700 Chromatography System Report Header

Sample Name
Sample Number
Operator
Interface #
AutoSampler
Rack/Vial
K411
9S190
5	Channel
None attached
0/0
Time
Studv
8/30/89 9:01 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition
Delay Tims
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
In.i. Volume :
Sample Amount :
Noise Threshold!
D i1u t i on Fac tor s
D i v i sor	:
T ime»
0.00
70.00
1.0
8/29/S9
min.
min.
pts/sec
11:40 PM
C:\2700\GC5\MCF5032. raw
C:\2700\GC5\MCF5032A. rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD. pre
C:\2700\GC5\MCF51B.smo
C:\2700\GC5\MCF54B. ssq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area fte.jec<
Area Thresnold
Mu11 i p1i er
Additive Constant
(.). oo
100
0. 67
. 00
Sun-~h Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier (3-as
Flow Rate
Sp 1 ,i t Ratio
T amperaturs
In j ec 11on Temp
Detector 1
Detector 2
Notes
3400 -
ID .23UMFILM
VARIAN
. 25MM
30M
HE
20CM/SEC LINEAR
rtx:
VELOCITY
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 32
*****
EXTERNAL STANDARD REPORT
Ret Time
Cmin]
Component
Name
Adjusted Amount Peak Area
ug	CuV-sec]
Peak Ht
C uV :
Raw Amount
uq \L
¦1 '11 31 D-BHG
SI. 23 ALDPl IN
-+~
*>5-
-&-.<> 5-
a. 42-
-34^=
22. 47
r
-»Q OA B-rui naMC

¦GHLPAMS-

	504. <:*>-
—¦ 2128*50-
—13411 00
—32. 19
162.30
130 i50
45.14 200091.22	16272
-171.
*r54
, 1,,_ .>>

~ « S-
i.70 ENDRIN
Q0Q068
0.94
1220.T"?
~9.02'
I.
I

-------
¦10. 71
	
r->innn n crn.Tf
	3.66
0 "*1
5779,00	

	
*19.82
ENDKETQ	
—— —
— '168 	

	
-------
FilaNut : C:\2700\6C5\nCFS032.raw	Date) 8/30/39 9:02 AH Page 1 of 1
Start Tiaai 0.00 tin End Tint* 70.00 ain low Points SZ38 uV High Point: 42669 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 «V Plot Scale: 100 aV
ChxoiatogTai
I R fc 5 $
«•' * 9 n m
^9 seas* i aa a s s? ?
a r RHaa*** 9 : r snn&as s
«f*o
>c»4 '
TT	TT
n
iDiiinnTurm—nn:1 n n
-ri-ir .11T
I I II Ml •
n i
A f f
- M
3 S S - 5
JL—u-jA

\ *
I i
r i . . . r
1LH	23.23	35.00	tt.tf	58.33
Tiu (ain)
000070

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SH£ET
Contract: 68-03-3249
fcPA SAMPLE NO.
L4A07
Lab Names LQCKHEED-ESC
Lab Code:	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
"/. Moisture: not dec. 0 dec. 	
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: CY/N) Y pHs
CAS NO.
COMPOUND
3AS No. :	SDS No. :
Lab Sample ID: 9S183
Lab File ID: 	
Date Received: 7-23-89
Date Extracted: 7-31-89
Date Analyzed: £'3o-£"
Dilution Factor:
CONCENTRATION UNITS:.
UP/kq	0
319-84-6	
319-35-7	
3 19-86-3	
58-89-9	
76-44-8	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9-	
72-54-8	
1031-07-8	
53494-70-5	
3103-71-9	
5103-74-2	
8001-35-2	
12674-11-2	
11104-28-2	
11141-16-5	
53469-21-9	
12672-29-6	
11097-69-1	
11096-82-5	
-alpha-BHC	
-beta-BHC	
-delta-BHC	
-gamma-BHC (Lindane)	
-Heptachlor	
-Aldr in	
-Heptachlor epoxide	
-Endosul-fan I	
-Dieldr in—	
-4,4'-DDE	
-Endr in	
-Endosul-fan II	
-4,4'-DDD	
-Endosul-fan sul+'ate	
-a,4'-DDT	
-Methoxychlor	
-Endrin ketone	
-alpha-Chlordane	
-gamma-Chlordane	
-Toxaphene—	
-ArocIor-1016—:	
-Ar oc 1 or -1221	
-Aroc1or-1232	
-Aroc lot—1242	
-Aroclor-1248	
-Aroc1or-1254	
-Aroclor-1260	
160
U
160
U
1 oO
•J
160
U
160
u
160
IJ
160
¦J
160
u
320
u
320
•J
320
u
320
u
320
u
320
IJ
320
u
1600
u
320
u
160
u
160
u
3200
IJ
1600
u
1600
u
1600'
IJ
1600
u
1600
u
3200
u
3200
u
FORM 1 PEST
1/87 Rev.
QOCC* I

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : L4A07
Sample Number: 9S183
Operator :
Time
Study
8/30/89 2:01 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
12:12 PM
Raw Data File
Result File :
Instrument File:
Process File.
Sample File :
Sequence File :
Inj. Volume :
Sample Amount
e:\pkd\MCFR0 3 0.raw
e:\pkd\MCFR03 0.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
R«c T1m
[mini
Coc^ontne
Adjujced Aoounc Raw Anounc Paak Araa Paak He
UC/K&.	uc/K6« [uv-..c] [uV]
MULTIPLIES
AdJ/Raw
a.t> e »H6
i. ¦ aa
ii>< unaa.aa wm.»
?i*0 I1CTBPBM
a.a» amoi

i.aa »«).» isaa.aa
¦ 9 i >6 m>0».8B	H
in 94 nrnnarii
ite.n
oot i
«> »H»iM

ItM.lS
tlH.il
j.ajn
n.ia bbt
n a« rvruin
¦u*.
"TTTOTO"
>!»¦»
j n aoaaa.nn »>i ai
Hibb mattiBB
23.63 DBC
123.33
184.10
2.43*6 37393.99
a. tt
0-67
»i6t '
¦\J(~
¦
• ^
U.51 " r
0,6?	V(«.
V<
0.67
Total Arta • 93504696.00
Total Concentration • 2468.7*98
Report by Tim Rand, Lockheed-ESC
000072

-------
Filename : e:\pkd\MCFIt030.rau	Date: 8/50/89 2:01 PM Page 1 of 1
Start Tine: 0.00 aln End Time: 47.00 iln Lou Point: -2117107 uV High Point: 2085350 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 iM Plot Scale: 250 mV
Oj
cr>
cz
o
cn

250.000-
208.333-
166.667-
125.000-
83.533-
41.667-
-0.000-
JO ^ \s
H kiS r—• tr
t- ad *— es
ol «"5 r—"
«=»
CN
s is
uS ocS


Tr-r^r
t I
<-> s 2 T- oE
~ H S s
I . lTj »
I I I
H l^i I i~*f I'T' I 'FY
cs
<2
E§£
i I r*J
15. 67
Ft"T
S

I i fr i I I I j I I I I I I I I I | I I I I I I I I I
31.33	39.17
I I I I
7 .83
23 . 50
Time (min)

-------
Nelson'Analytical 2700 Chromatography System Report Header
Sample Name : L4A07
Sample Number: 9S183
Operator :
Time
Study
8/30/89 2:40 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range : 10000
Varian 8000 without controller
255/255
Data Acquisition	Time: 8/30/89 12:12 PM
Delay Time :	0.00 min.
End Time	:	47.00 min.
Sampling Rate :	1.0 pts/sec
Raw Data File :	e:\pkd\MCFR030.raw
Result File :	e:\pkd\MCFR030A.rst
Instrument File:	e:\pkd\pkd.ins
Process File :	e:\pkd\pextstd.prc
Sample File :	e:\pkd\clpb.smp
Sequence File :	e:\pkd\MCFRLND.seq
Inj. Volume
Sample Amount
2 uL
1.0000 uL
Area Reject
: 0.00
~EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat TLm	Cooponoac	Adjusted Aoount Rav Amount Peak Area Peak He MULTIPLIER
(tain |	Nana	UC/fcfc	[uV-s«c] [uVj Adj/Rav
9\U * frftftWTI
—10.a* 008
^j.au &HPMU
rn it nnn
25.65 0BC

80130
i30 QfiifOI 09 iQBBO.tU
US.04
1060.56

¦JI300.83
3011 00
ffUl.J>
i f.aa.Ta
L.3888
j.03a?
i.aam
»i98
147.38
I9ii9
219.96
2.45«6 57393.99

w<-
9,67
-VL-
8ifcJ
0.67

d.ef
01 §?
Total Araa - 231543424.00
Total Concentration • 10531.4482
Report by Tim Rand, Lockheed-ESC
000074

-------
„	. Chromatogram
FlteNane : e:\pkd\HCFH030.raw Date: 8/30/89 2:41 PH	Page 1 of 1
Start Tim: 0.00 ailn End line: 47.00 "In Lou Point: -2117107 uV	High Point: 2085350 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 MV Plot Scale: 250 mV
in in g Lfi
i/S r—" oi
52 St. R ES ^ ^ \£
c
cz
o
C2i.
CO
CU»
o=;
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
CN	CM r\l	CN
H3
r~r^T

t I
h* ^
m as
-rV+r
v
-£-3-


a
I "I i I I I I [i I I i I I i I i*1 I I I I I I Ti I | I I i I I I I I I | I I I I I
7.83	15.67	23.50	31.33
Time (min)
I l i | i I l I I l l I l
39. 17

-------
	_Nelson Analytical_27QQ Chromatography System Report Header
Sample Name : L4A07
Sample Number: 9S183
Operator	:
Time
S tudv
8/.30/39 ~:4Q AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Timie: 8/29/89 6:43 PM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
In j. VoIume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0. ("JO
70.00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5028.raw
C:\2700\GC5\MCF5028.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seg
2 uL
1.0000 UG/kg
1
1. <50
1.0000
Area Reject	s 0.00
Area Threshold J 100
Multiplier	: 0.67
Additive Constant: 0.00
8uni:n Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flaw Rate
Sp1i t Rat io
T emper ature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400-b
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
160 1/MIN TO 230
200
300
15 PSI
Total Number of Peaks Detected: 69
Re t T i me
[min ]
Componen t
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\|^jj	CuV-sec3
Peak Ht
CuVJ
Raw Amount
uq\L
-7-s G-BHC
AO. 15 IIPTCIILK
5.01	5*4-52.00
2114.71
i 09
—24ii.00
2119.50
24. 13
134.Su
-48
-Jr3-
I
11.22 />LDRIN
'¦>. -j -ii
tt
Sa.OO HEPEFQX
0.34
1441.81
-111.81
"51
g9v9<3-CNDQl
33 >90 OIELDHIN
¦30-
r92-
1494.00
1951.01-
134.
*-rr
-171.22
000076
r. 37
f

-------
304 16 CND02	210.01 720000.00	72306>00	311.61 'ffH.
41.16 CNDALD	0.25	344.00	41.00	0.37 £
46.05 DDT	12. 15	28141.97	2445.46	18. 10
551 05 METHQXV	err*Q	J350i 70	102.01	9.07" J'M
SI.43 DBC	186.46 267625.22 23765.01	278.29
Total Area = 1057258.63
Total Concentration =
Report by Doherty Bresnahan
000077

-------
FileNaaa : C:\2700\GC3\MCF3028.ra»	Data: 8/30/89 7:49 AH Pa 100 «V
Chromatograa
J a 9*¦ tSM
^p. j
	
ftfS set s?s»sr« r s?	a
39 KB* *£K JIRHBtm? 5 :r CDBDBC-asa 4
I «H
it	3
u	3
" -~_a
3
»4
s ji , iii,
» j i 1 i 1 li
i ff.. . " i . r. ?i i it r.
£ '4
f. . ¦ *
11.67
23.33	9.00
Tiia (ain)
*.W
58.3
000078

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
Inter-face #
AutoSampler
Rack/Vial
L4A07
9S183
5	Channel
None attached
0/0
Time
Study
8/30/89 85 50 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition Time* 8/29/89 6:43 PM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
In,i. Volume
Sample Amount
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC3\MCF5028. raw
C:\2700\GC5\MCF5028A.rst
C:\2700\GCS\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF31B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 UG/kg
Area Reject
. 00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
0.67
0. (50
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument	:VARIAN
Column	:	.25MM
Column Length	:	30M
Carrier Gas	s	HE
Flow Rate	:	20CM/SEC
Split Racio	:
Temperature	:	160
Injection Temp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400-5
ID .23UMFILM
RTXI
LINEAR VELOCITY
PS I
1/MIN TO 230
Total Number o-f Peaks Detected: 69
**********
EXTERNAL STANDARD REPORT
Ret Time
C m i n 3
Component
Name
11.77 B-BHG
<>4.25 D DUG
Adjusted Amount Peak Area Peak Ht Raw Amount
ug\L,-,	CuV-sec3 CuV3	uq\L
-J>4-
M I [J
01 ii'T'
792«00
:ZB1.29
—00179
0.50 v


-rrrSi
21.22 ALDPIH	
aa.q7Q-CM^PAME
211?.CO
6593.00
134.G6
483.43
30.95 A CIILDANC
-5 1 ¦ 53 DDC
. ja
1.51
rrr-42-
-211-3-. 00-
-236.22
-t~07'T62"-4^'7 [s

0i 62	2^^

-------
3u« 63
CNDKIH	
r\r\r\
	5-.02
	6S49.47
	452.06	









0 • 06

1 «
-------
FildtaM : C:\2700\6C3\HCF3028.ra*	OaUt 8/30/89 8:31 AN Pap 1 of 1
Start Tinai 0.00 ain End Tina* 70.00 ain Low Point: 3246 uV High Point: 610825 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 »V Plot Scale: 100 aV
Chxe*atogxa»
ltfl
a 3 HI fcSSM? M3 55fta:«»tSKK 5?	i
?5 JCS9 RCX 3&R RR R RR R9 8 J5 { KB BUI S3 II 9
3~ irfmroiaii mwiif'u niiirriiii'ft
ii •	hi
"VftfflTSWn f; mi Kiaiii;';; :;:1
ni
^lA.
II 5 o
,i, I
¦M I ^ I-I I I I Hi | I I I H
11.(7
23.3)
35.00
Tilt (ain)
44.(7
58.33

000081

-------
ID
PESTICIDE 0RGANIC5 ANALYSIS DATA SHtET
fcPA SAMPLE NO.
LSI 3
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Codes	 Case No.:
Matrix: (soil/water) SOIL
Sample wt/val: 30 grams
Level: (low/med) LOW
V. Moisture: not dec. 2.4 dec,
Extraction: (SepF/Cont/Sonc)
6PC Cleanup: J
-alpha-Ch lardane		164	U
-gamma-Chlordane		164	U
-Toxaphene		3279	U
-Aroclor-1016		1639	U
-Aroc lor-1221		1639	U
-Aroclor-1232		1639	U
-Aroc lor-1242		1639	U
-Aroc lor-1248		1639	U
-Aroc lor-1254		3279	U
-Aroc 1 or-1260		327?	U
FORM 1 PEST
1 i37 Rev,
OCCCA a.

-------
Sample Name : L513
Sample Number: 9S192
Operator :
Nelson Analytical 2700 Chromatography System Report Header
4:28 PM
Time
Study
8/31/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time:	8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0	pts/sec
6:12 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR03 7.raw
e:\pkd\MCFR037A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\fltott
IVMCre
e: \pkd\F
2 uL
1.0000 uL
, seq
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT4
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
[ata)
Adjuacad taouac Raw Aaouac Paak Area Paak Be MULTIPLIES
UG/ft£	UC/|C£ [uV-sacI [uV] Ad j/Raw
a n r.nnnmt
» CttBMIE
19.«< BBS
H.H BOO
2i n nraonnim
23.67 OBC
(i ai
i.a» naan,a9
T98.H

iitt tl?B97.ii 5006.a>
9,»*
ifc.it a«»7B.aa imui
»¦»
9».89
1 j fcOai *3161.aa
17 1
at.ei aauMiaa imaitt
138.62
327.38 3.88a6 123916.93
11 <9
0.00
a.ta


0.60
8.«i

V/IL
0.69
Xozmi Ar«* - 81S4X26.50
Cene«acsMleo m 460.&516
Report by Tim Rand, Lockheed-ESC
000083

-------
Chromatoqram
FileName : e:\pkdVHCF8037.rau	Date: 8/31/89 4:28 PH Page 1 of 1
Start Tine: 0.00 sin End lias: 47.00 Bin low Point: -1721507 UV High Point: 1993660 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 uV
250.000-
208.333-
166.667-
(U
r~ 125.000-
cry
o_>
CtZ
63.333-
o
o
.667-
ae
&
-0.000-
oa ho oa
		„ 		H~> hO CT>			. _
3;* 33 ^ ^ :=• ^
•—	• «—	CNI	CM
n^rW/V-ir
	
I * * I	I	I
c_> o
I I
I


c >
»
u >
I I
I I II
f3! I I I I l^p I 1^ I Fj
I I I I I I V-1! I
&
r^-
i i-r i i i i i i | i i i i i i i i i | i
i i i i

-------
Sample Nana
Sample Number
Operator
Interface #
AutoSampler
Rack/Vial
Nelson Analytical 2700 Chromatography System Report Header
4:02 PM
L513
9S192
Time
Study
8/31/89
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time ; 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
6:12 PM
Rav Data File	:
Result File	:
Instrument File:
Process File	;
Sample File	:
Sequence File	:
Inj. Volume	;
Sample Amount	:
e:\pkd\MCFRQ 3 7.raw
e:\pkd\MCFR0 3 7.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e: \pkd1		
e:\pkd\MCFRLND.seq
2 UL
1.0000 uL
Area Reject
0.00
~~~~~EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa	Cuapooant	Adjuatad Aaevnt Haw tmnt ?«ak Ana Fiik Ht MULTIPLIER
tola)	Hum	UC/|&	UC/|CA tuV-»ae| (uV) AdJ/fUv














23.67 08C
300.14
441.39
3.8«a* IZ3916.93
3.63
¦ W'fc
— VK
WC
Total Axaa - mSMl.OO
Total Caaeaatcatioa » 334.4402
Report by Tim Rand, Lockheed-ISC
isssassss
V
000085

-------
Chromatoqram
Filename : e:\pkd\HCFR037.rau	Date: S/31/89 4:02 PM Page 1 of 1	7
Start Tine: 0.00 Bin End Has: 47.00 Bin Lou Point: -1721507 uV High Point: 1993660 uV
Vertical Scale Factor: O.OO Plot Offset: 0 MV Plot Scale: 250 oV
OQ K") oa tji
3 S SI 1
250.000	
200.333
166.667
125.000	
CO
CXL
83.333	
-0.000	
7.83	15.67	23.50		31.33	39.17
¦P(

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : LSI3
Sample Number: 9S192
Operator	:
Time
Study
8/30/89 3:10 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
0
None
0/0
Channel
attached
A/D mV Range s 1000
Data Acquisition
Delay Time
En d T i me
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount
Noise Thresholds
Dilution Factor:
D ivisor	:
Time: B/30/99 3:23 AM
0.00 min.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5035.raw
C:\2700\GC5\MCF5035.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A. amp
C:\2700\GC5\MCF54A.seq
2 uL
I.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Mu11 i p1i er	: 0.68
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T erftoer at u.re
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400 -S-"
.2SMM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY II
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 71
**********
EXTERNAL STANDARD REPORT
Ret Time
Cm in 3
Component
Name
Adjusted Amount Peak Area
ug	CuV-sec1
Peak Ht
CuV 3
Raw Amount
u.q \L
1 ?
1 o
JV2-
oia
ijmBHC	__
UDTPLII C.
	0. 04—
	—
	12!29	
	0. 0 6






	n—TT

w
ucDccnv


• i /


n o
r*Mnn 1





r94-
PIELBEIN			
	—
-^•24-rS9—
—205¦73	
	a*
000087

-------
?S. 17
ENDQ3	
	¦«.&9	23-V9&^35	1361. 01	
	101 1 'V
1
* L. C 4
r>r>*r


<=¦ L. OA
Merunvv
1 00 l'")l9 'i? 'Ir't
L-
61.77
DBC
2813.81 3.97a6 131955.50
4137.95
J
LjW
t
Total Area = 4020418.23
Total Concentration - 2829.2379
Report by Doherty Bresnahan
000088

-------
FileNut : C:\2700\6C3\MCF3033.rw	Oatas 8/30/39 8M1 AH Pa?* 1 oi 1
Start Tiae* 0.00 ain End Tiaas 70.00 ain Low Point: S2SS uV High Points 187885 uV
Vertical Scale Factor: 0.00 Plat Offsets 0 aV Plat Scales 100 aV
Chromatogra*
ltNH
aa-j
««-:
I
| wrg
¦n
at
3.8H
k.w-4
fe is s"? a J* s sm«=R setie	ssm r sua
- MS S 8* t BfcEJlRB* *¦*; 55555 a (Hill a 8ft I
Vnnnrunrnr niririmrf • ^
'••Trrrrj
* f j I | | I | 6 la
¦'I 11 *, i ft. i. 11 fi i "i 1.3 i «•¦ 11 "¦ i	r . q
11(7	8.33	35.01	H.U
Tii» (ain)
5».a
000089

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : LSI5
Sample Number! 9S192
Operator
Time
Study
8/30/89 9:07 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range s 1000
Data Acquisition Timet
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
In j. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
8/30/89
0.00 m i n.
70.00 min.
1.0 pts/sec
AM
C:\2700\GC5\MCF5035. raw
C:\2700\GC5\MCF5035A.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF34B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Ra.iect	: 0.00
Area Threshold : 100
Multiplier	: 0.68
Additive Constants 0.00
Bunch Factor: l
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
3p 1 i t F:at io
T smperature
In j ec 11on T smp.
Detector 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
15 F'SI
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 71
Ret Time
Cmin 3
**********
Component
Name
EXTERNAL STANDARD REPORT """""
Adjusted Amount Peak Area Peak Ht Raw Amount
ug	CuV-sec3 CuV]	ug\L

_A—StHG—...
D 01 tC
21.71 ftLDRIM-
1*2. 12
39.03 G—CHUPANC
il.00 fl-GHLDf\NE
¦3 '1. 5T DDE
0.14
945.38
0.11
0. 10
260. 00'
595«00-
¦*2.-23
63. 17

2. 39	11831. SI

2-15 i)
-5-t
r-04-
—tlH
12.08

1 i Ol
52738.2S
607.12
4042.'
OLI
17.76
I
a
' S>
ooooao

-------
36. 73 ENDRIN	'3.16 <1065.58 3151 G1	4i66 ^
"10.50 DDD	9.58	1')927. 28	958.36	14.0
-------
FiltNaat t C:\2700\GC3\flCF3033.raM	Dates 8/30/89 9:08 AN Pa*« 1 of 1
Start Tia«s 0.00 ain End Tiati 70.00 ain Low Points S2S3 uV High Points 18788S uV
Vertical Scala Factors 0.00 Plat OHsats 0 aV Plot Scala: 100 aV
Chroaatograi
mm-.
ItJlH
Kj®4
'».«H
3St4
M
ilW-3 !
31
34-Yrr*i
j>s»-3 ' ""
a *s CSV a as 8 sm*=6 sws sssas;* ssj« c. as*
- »- *?j « ss c bkbhab* hp*; ?:s;rs phiibb a saa
sn
JJLi-
7f--Trw
1,	il? S, 1	_»
11(7
23.33	35.00
Tii* (aia)
n.a
B.33
000092

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
t£PA SAMPLE NO.
M14A08
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Code:	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 0.4 dec. 	
Ev.tract ion: (SepF/Cont/Sonc) SONC
GF'C Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:——— SDG No.:
Lab Sample ID: 9S1S4
Lab File ID: 	
Date Received: 7-23-39
Date Extracted: 7-31-89
Date Analysed:	£ "I
Dilution Factor:	10
CONCENTRATION UNITS:
Llfl/k'3
319-84-6	a lpha-BHC		161	U
319-85-7	beta-BHC		161	U
319-86-8	del ta-BHC		161	U
58-89-9	gamma-BHC (Lindane)		161	U
76-44-8	Heptach lor		161	U
309-00-2	Aldrin		161	U
1024-57-3	Heptach lor epoxide		161	U
959-98-8	Endosul -fan I		161	U
60-57-1	Dieldr in		321	U
72-55-9	4, 4'-DDE		321
72-20-8	Endrin		321	U
33213-65-9		—Endosul-fan II		321	U
72-54-8	4, 4' -DDD		321	U
1031-07-8	Endosul-fan sulfate		321	U
50-29-3	4, 4'-DDT		321	U
72-43-5	Methoxychlor		1606	U
53494-70-5	Endrin ketone		321	U
5103-71-9	alpha-Ch lor dan a		161	U
5103-74-2	gamma-Ch lordane		161	U
8001-35-2	Toxaphene		3213	U
12674-11-2	Aroc lor—1016		1606	U
11104-28-2	Aroc lor-1221		1606	U
11141-16-5	Aroc lor-1232		1606	U
53469-21-9	Aroc lor-1242		1606	U
12672-29-6	Aroclor-1248		1606	U
11097-69-1	Aroc lor-1254		3213	U
11096-82-5	Aroc lor-1260		3213	U
FORM 1 PEST	1/37 Rev.
ct 00c'3

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator ;
Interface # :
AutoSampler :
Rack/Vial :
M14A08
9S184
Time
study
8/30/89 2:03
MCFARLAND
PM
2	Channel : 8 A/D §V Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
1:03 FM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e s\pkd\MCFR031.raw
e:\pkd\HCFR031.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: " Varian 3400-1	GC Column ID: 2250/2401
Rat liam Coapanuie	Adju»t«d Aaouac Raw Amount Puk Ana Paak Be MULTIPLIES
(alnl	Haaa	UG/K&.	U6fl0» tuV-s.e) [uV] Adj/SUv
% n *tnam.
I.na HBfEWJl
».»	8SB8i —
in it rirnniiTH	
Ell—
	If»## OPT
23.7* DSC
>>.aa
¦Ji >Q88J>.88 8>!8>.a»
24, HI
jb.i2 /kmt.n muM
H)il>

t.aawfl 88*18.«i
imaa.ja
IBM
	5>8i»*
sa.i» >k»3».i)J—mua.M
121.10
	
181.0*
I.IW IWtli Tt
Ml«< 30280.91
a.*?
mn—v<-
. \ff-


B'i'BT
0.67
. vf~
. :•>
Total Axaa - H06J*««.00
Total ConcanttatLsa •
Report by Tim Rand, Lockheed-ISC
000094

-------
Chromatogram
FIleNane : e:\pkd\MCFR031.rau	Date: 8/30/89 2:03 PH Page 1 of 1
Start Tim: 0.00 mln End Time: 47.00 aln low Point: -1908977 uV High Point: 1214870 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 HV
CL>
cr>
cr»

cm
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
3 c-4 ^9 3 K a! 3 >—5	^
f«-j ? ? s> p s s s
—1	vH r— crJ	3
CN	r«"j •--»
&
2 - g
& S s
I	I I
s
I i i in I i3? i I f3! I I I f-f~T Pi T

i i i i i i i i
7.83
15.67
23.50
Time (min)
rl I l i I | I I I I I l I I I j l I
31.33	39.17
I I I I I

-------
Sample Name : M14A08
Sample Number: 9S184
Operator :
Nelson Analytical 2700 Chromatography System Report Header
2:43 PM
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
1:03 PM
Raw Data File	:
Result File
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 31.raw
e:\pkd\MCFR0 31A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
0.00
***** external standard report*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tim*
Cooponant
Adjuatad Amount Slav Amount ?aak Araa Paak He MULTIPLIER.
Bta)
Nana


UC/|t£,
[uV-iae)
(uV)

Adj/Raw












































- t/*-























































23.7*
DBC
144.
.92
216.31
2.41.6
50290.91
0
.67
Total Araa - 11333606.00
Total Ceaeaaeracloa » 487.3330
Report by Tim Rand, Lockheed-ESC
0000U6

-------
_	Chromatogram
HleNaae : e:\pfcd\HCFR031.ra« Date: 8/30/89 2:43 PN	Page 1 of 1 ^
Start lime: 0.00 "In End Times 47.00 Bin Lou Point: -1908977 uV	High Point: 1214870 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nN Plot Scale: 250 MV
gj	to lt> r-^ gj in ^ pj
CN -P S K oi	IT) id
IC 3»
J*
_ _ .	co erj ¦=> en
r —'	wJ r—" er»	iq 
o_>
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000
if
¥ ^
¦ ¦ * CD
i i
v ^ H e
fr .	. ¦ ~
a
i i r~i t*i i i i pT i i^r » it i r~j i i i i i i y-1! i | i i*t i i i i i i | i i i i i
7.83	15.67	23.50	31.33
Time (min)
I | i I I I I I I I 1
39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M14A08
Sample Number! 9S184
Operator	:
Time
Studv
9/30/89 7:51
MCFARLAND
AM
Inter-face #
AutaSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Ranqe : 1000
Data Acquisition Times 8/29/39 7:57 PM
Delay Tima	: 0.00 min.
End Time	s 70.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5029.raw
C!\2700\GC5\MCF5029.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF34A.seq
Ini. Volume
Samp 1e Amoun t
2 uL
1.0000 UG/kg
Area Reject
0. 00
Noise Threshold
Dilution Factor
D i v i sor
1
1.00
1.0000
Area Threshold
Mult ip1ier
Additive Constant
100
0. 67
0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400- <3
. 25MM ID .25UMFILM RTX5
30M
HE
20CM/3EC LINEAR VELOCITY
='SI
160
200
300
1 /MIN TO 230
Total Number o-f Peaks Detected: 123

Ret Time
[min]
*********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amoumt Peak Area
ugNJUL t\bL/ CuV-sec3

Peak Ht
CuV3
Raw Amount
up \L
12.39 G-BHC	
17.00 HPTCHLK	
£Jr, 52--AUBB-I-N	
•"» jL	UCPCP.ny
~ ¦ VC I IL. I ^ I 'J M
7ft. 14 EN0Q1	
83 DIELDRIN
1. 10
1.02
6625»18
5266,. Ql
'). 36	27399. 77
463<33
1 't73. on
1635a 00
-as
'379S7. 7°
iaOfl. 41
oouoaa
^ i
17153. 37
1305.21-
1. 64
Srf
-50
12 i-2-t1
$
c
i

-------
3B.12 EIMD02	S-^6—29565. SO	2182. 11	13. 93 V,
>1.12 ENDALD	&*-S9	11663.45	792. 75	12.50
05.98 DDT	54. 46 127754i75	11491. 77	01. 20. ^
36.13 METHQXY	16.'55	7112< 59	599^20	24
61.35 DBC	182.16 261454.11 23415.46	271.88

Total Area = 586418.88
Total Concentration - 308.3305
Report by Doherty Breanahan
000099

-------
FileNut : C:\2700\6C3\flCF5029.ra*	DaU« 8/30/89 7:53 AM ?ag» 1 of 1
Start Tint: 0.00 tin End Tim: 70.00 ain Lot* Point: 5268 uV High Point: 63569 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 oV Plot Scale: 100 «V
Chrciatograa
I
¦w
U
5
J n lascs	sas«i!3WP;*5i!si?5S«iera jwar saassw
.>1 *k*o» ssiSSiTt ZXKR8»AXRMRM:S;5SS?a RRFXK Fa81S&33
• M ¦ « l« MM Mi I WIMII IHM1I •• Ml lilt I t II I l«M IHMHMKtll IIIIMH lllltl •••*• M IM M» »•«»<• III!
-J I!
3-1'iVrnrr nip
!«a-3 '
* I I
3f I - i - I a 2
!i » j s I ¦ 1 j
ii, i
11.67	23.33	33.00	1l.il	58.33
TiM (mm)
000100

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M14A08
Sample Number: 9S184
Operator	:
T ime
Study
3/30/89 8:5:
MCFARLAND
AM
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time* 8/29/89 7:57 PM
Delay Time	:	0.00 min.
End Time	:	70.00 min.
Sampling Rate :	1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C: \2700\GC5\MCF5029.raw
C:\2700\GC5\MCF5029A.rst
C:\2700\GCS\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
Ini. Volume
Samp Ie Amount
2 uL
1.0000 UG/kg
Area Reject
: 0. 00
Noise Threshold
Dilution Factor
D i v i sor
1
1.00
1.0000
Area Threshold
Mult ip1ier
Additive Constant
100
0.67
0. 00
Bunch Factor: 1
Instrument Conditions
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T emperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400 — S*
.25MM ID .25UMFILM RTXS
30M
HE
20CM/SEC LINEAR VELOCITY
PS I
160
200
300
1/MIN TO 230
Total Number o+ Peaks Detected: 123
**********
EXTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount
F'eak Area
C uV-sec1
Peak Ht
CuV]
Raw Amoun t
uq\L


-BHG-
t1.60 B-BMG

n-RHr.
—».-i+-
38.-90
4. Z(t
952.00
143.21
90970.00-
-406-ItOS-
1	I 'JT
21.52 mLOBIN	
20.97 0' 'CHLDANE
-4-r^J
27099.77

r£*A-
30.94 A CI ILDANE-
Q0Q101
-4-2-57-
1 1.29
-6527-1-1-59-
>37213.25
3436.06
^XoTi
¦¦gs. .nja
i-SW>
-oa 09

-44-59-.-75- -
18.77
-46.05
_ ii

-------
¦51.81 DDE ——	151.68 672327.50—578-29-. 47	526.-59- V, -
361 74 CNDHIN- 				t-3,i<>4	t-7022. 48	1141.94	l'"M"fc6
10.40 DDP 			i"5"«°09	23Q56. 16	1944.73	2'2.52
<4.55 gMPOSUUgATE	Z-.*M	1070^.92-- - -76»l-,4>8	&T-S9-
€i. 1? SMPKgTO	5^4-3	'1916. 19	563.01	\
61.35 DBC	231.42 261434.11 23413.46 343.40
Total Area » 1232967.00
Total Concentration ¦ 490.1710
Report by Doherty Sresnahan
000102

-------
FilefU* : C:\2700\6C3\nCFS029.raH	Date: 8/30/89 8:54 AH Pa^e 1 of 1
Start Tin: 0.00 ain End Tiaat 70.00 iin Low Point: 5268 uV High Point: 63569 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Cfcxoiatograa
5 SU9P 8.4 913 3
It RBPnft KaaSBMI
B a tifC* ft*?? S3 SS3t£8KfcZ.=*i=?3Seir:
. »	55555SE IXKMaMRRRR
•II
K
§
U
a
11.67
35.0B
23.33
Ti>* (tin)
000103

-------
ID
PESTICIDE ORGAN ICS ANALYSIS DATA 3Ht£ET
Lab Name! LQCKHEED-ESC Contract: 68-03-3249
t£F'A SAMPLE NO.
M4A06
Lab Codes	 Case No. »
Matrix: (soil/water) SOIL
Sample wt/voi: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 3.4 dec.
Extraction: (3epF/Cont/Sonc)
GF'C Cleanup: (Y/N) Y pH:
-r*3 NO.
COMPOUND
SAS No. :	SDCS No. :
Lab Sample ID: 9S182
Lab File ID: 	
Date Received: 7-25-89
		Date Extracted: 7-31-89
50NC	Date Analysed-'
Dilution Factor:	1<
CONCENTRATION UNITS:
HQ/k q	Q
319-94-6	alpha-BHC		166	U
319-85-7	beta-BHC		166	U
319-86-8	delta-BHC		166	U
53-89-9	gamma-BHC (Lindane)		166	U
76-44-8	Hep tach 1 or		166	IJ
309-00-2	Aldrin		166	U
1024-57-3	Heptachlor epoxide		166	U
959-98-8	Endosul-fan I			166	U
60—57— l	Oi^ldrin		331	J
72-55-9	4.4* -DDE		"31	'•_!
"*2-20—8—		Endrin		_;3i	l'
33213-65-9	Endosul fan II		T-..1	J
72-54-8	4. 4' —DDD		331	'J
1031-07-3	Endosul+an sulfate		331	U
50-29-3	4, 4'-DDT		331	IJ
72-43-5	Methoxvcnlor		1656	U
53494-70-5—	Endrin ketone—			331	U
5103-71-9	alpha-Ch lor dane		166	U
5103-74-2	gamma-Ch lor dane		166	U
3001-35-2	Toxaphene		3313	U
12674-11-2	Aroclor-1016		1656	U
11104-28-2	Aroc lor-1221		1656	U
11141-16-5	Aroc lor-1232		1656	U
53469-21-9	Aroc lor-1242		1656	LJ
12672-29-6	Aroclor-1248		1656	U
11097-69-1	Aroc lor-1254		3313	U
11096-82-5	Aroc lor-1260		3313	U
FORM 1 PEST	1/37 Rev.
CO o1 U +

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M4A06
Sample Number: 9S182
Operator :
Time
Study
8/30/89 1:56 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89 9:24 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
47.00
1.0
nun.
min.
pts/sec
e:\pkd\MCFR02 8.raw
e:\pkd\MCFR028.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tim*	Cooponaat	Adjuatad Anount Raw Anount ?aak Araa Paak St MULTIPLIER
(mln)	Nana	UC/fb	UC/)& [uV-sacJ [uV] Adj/Rav



















25.36 DBC
117.
.81
170.
. 74
2.27«6
33343.06
0.69
vs
Total Ar«* « 4645640.00








Total Concent radon ¦ 207.3449








Report by Tim Rand, Lockheed-ESC
000105

-------
„ ,	Chroraatogram
FileMame : e:\pkd\HCFR02B.raw Date: 8/30/09 1:56 PN	Page 1 of 1
Start Tine: 0.00 ain End Tiae: 47.00 ain Low Point: -2117657 uV	High Point: 956550 uV
Vertical Scale Factor: 0.00 Plot Offaat: 0 altf Plot Scale: 250 mV
DO
DO CO
a a
250.000
208.333
166.667
125.000
83.333
.41.667

-0.000
7.83	15.67	23.50	31.33	39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Nana : M4A06
Sample Number: 9S182
Operator :
Time
Study
8/30/89 2:37 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time:	8/30/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate : 1.0	pts/sec
9:24 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 2 8.raw
e:\pkd\MCFR02 8A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
*EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
!Ut Tiaa	Caoponaac	Adjuacsd Amount Raw Amount P.mk Area P.&k Ht MULTIPLIER
(Bin)	Haaa	UC'tt*	U6/9& tuV-sae] [uV] Ad)/JUw
¦oii» » amawg
•to.at DOB-
25.36 0BC
BIBQCWAM

11 ii aoeosi
t-r&-
?0.5»
iot.e»
.04»6 0*070.00
183 3M98.6I
b9i k9
aa»a> aix»i99
140.76
204.00
2.27«6 53343.06
r*9-
Qit*
0.69
t/fc.

¦/lt-
Total Arta • 4636240.00
Total Concentration ¦ 239.2634
Report by Tim Rand, Lockheed-ESC
000107

-------
Chromatogram
Page 1 of 1
HleNaae : e:\pkd\HCFR02B.rau	Date: B/30/B9 2:37 PH
Start Tine: 0.00 ain End Tin: 47.00 ain Low Point: -2117657 uV High Point: 956550 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 mv Plot Scale: 250 mV

CO

250.000-
20B.333-
166.667-
125.000-
83.333-
41.667-
O
o
Q.ooo-
C
QC

Cs CT>
o
ccS
CO
DO CO
in
m ~
i ill
IT
i 'i
vVrr~irr^V
!rr =j=
CD 9
_L •
I
§i e
I I I
I I I I j^T* I i*? I iuT1 l
&
I I I I I T'l I I I i^T* I I I I I I I I I I I I I I I I I » I I I I I I I I
7 . 83
m
mU-5V
t i mp t m i it)
Jl,


-------
Nelson Analytical 2700 Chromatography System Report Header
/ample Name :
Jample Number:
Operator
nter-face #
HutoSampler
J*ack/Vial
M4A06
9S182
5	Channel
None attached
0/0
Time
Study
8/29/89 5:03 PM
MCFARLAND
Jata Acquisition Time#
i
t
e1ay T i ma
n d Ti me
Sampling Rate
taw Data File
eault File
.nstrument File
Vocess File
~ample File
Sequence File
0.00
70.00
1.0
8/29/89 3:02 PM
min.
min.
pts/sec
A/D mV Range
1000
C:\2700\GCS\MCF3026.raw
C:\2700\GC5\MCF5026.rst
C:\2700\GCS\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC3\MCF54A.seq
inj. Volume
Sample Amount
2 uL
1.0000 UG/kg
Area Reject
0.00

loise Threshold
ilution Factor
ivisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
0. 69
0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Splift Ratio
Temperature
I n ,i ec t i on T emp
Detector 1
Detector 2
Notes
VARIAN 3400 ""D
.25MM ID .2SUMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number ot Peaks Detected: 41
BCTERNAL STANDARD REPORT
\et Time
Cmin ]
Component
Name
Adjusted Amount Paak Area Peak Ht Raw Amount
ug\^	CuV-aec] CuV]	ugXs.
5-t. 2-7-AkDRIN—
.26.21 HEPEPQX
30.02 CNDQ1
73.07 DICLDPlIN
-30. 19 CNC02	
'11.16 ENDALD	

-2247. 00-
2077.00

0. 72
-0. 47
-7-730.00-
1401.50

O. 57
oooioa
773. 50-
1 TO —»—
1 %/ii • *- ¦->
-281.33
¦A1
4-25.09
—67.44
-?2.-9

-------
'16. OS DDT	1 *1 19	525151 02	2075. 27	20. 56
55i0l METIIQXV	10.9-1	5944.50- 592.44	15. Ql-
61.37 DBC	162.40 226342.03 19901.02	235.37
Total Area = 276380.56
Total Concentration = 191.1024
Report by Doherty Bresnahan

000110

-------
FileNaae : C:\2700\6C3\HCF302i.raw	Data: 8/29/89 3:06 Ptt Pap t of t
Start Tioei 0.00 tin End Tioa> 70.00 ain low Point: 2198 uV High Point: 45492 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Cfcxoiatograft
i t;? s 8 ft ?s It8t 21 a ss *
s ;i> i ri c	ug i
-mrrnr'niTi mm hi mi I'm n rmi imi n
K iiiilii e
4—* S, ? h, —L
1111
54.33
11H	23.33	35.09
TIm (aia)
OOOlll

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : M4A06
Sample Number: 9S182
Coerator	:
T ime
Studv
3/30.-59 3:0-3 AM
MCFARLANC
Inter-face #
AutoSampler
Rack./Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Time: 8/29/39
0.00 m i n.
70.00 min.
1.0 pts/sec
3:02 PM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5026. raw
C:\2700\GC5\MCF5026B.rst
C:\2700\GC5\FOE.ins
C:\2700\SC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
Inj. Volume
Sample Amount
2 uL
1.0000 UG/kq
Area Reiect
V. 00
Noise Thresnold
Dilution Factor
Divisor
1
1. <30
1.0000
Area Thresnold
Mu11 i p11er
Additive Constant
100
0.69
0. 00
Buncfi Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sol it Ratio
T siiiBerature
In.iection Temp
Detector 1
Detector 2
Notes
y'ARIAN 3400
.25MM ID .25UMFILM RTX3
30M
HE
20CM/SEC LINEAR VELCC IT.' 15
160 1/MIN TO 230
200
300
Total Number o-f Peaks Detected!
41
***«
0CTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount Peak Area
A, CuV-sec]
Peak Ht
C LlV ]
Raw Arcant
US'TL
JL ± t
ALPftitj	

	¦ T'Q
	2247.00
	132.23	

*7 f





i ii 1
— a er .1
r-k^r-




nn'nn 1





i* 'T v U * • » w
... i.. - |
_'W • /
ENDRIN

I™. ti?s
132S^14
1 !3
-» 4 tr
t


000112



1
I

-------
44. oa CUDOGULrftTC	&r	1229.00 55. 27	
51.04 CNDKCTO	0. .30 455i 00	39. 33	0.44
61.37 DBC	206.32 226342.03 19901.02	299.01
Total Area = 536884.13
Total Concentration = 279.9784
Report by Doherty Bregnahan
ooona

-------
FileNaaa : C:\2700\GC3\HCF3024.ra*	Date: 8/30/89 8:49 AH Pigt 1 of 1
Start TiM< 0.00 ain End Tia»» 70.00 ain Lon Point: 51?0 uV High Point: *5*92 uV
Vertical Seals Factor: 0.00 Plat Offset: 0 aV Plot Scale: 100 aV
Chromatogram

*iG
* ; «a t ss k as a ss *t* *
; sa e ri r mi$;s ::»b re its i

i—mi ,iii iimi imn ,11111 mini i'ii! 11 I'nntfnr
« 1 1
n %
II _ i. i 1
•H 8,5 8 *, ,'r
11.67
23.23
35.00
Titt (tin)
#.W
58.33
000114

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
t£PA SAMPLE NO.
M510
Lab Names LQCKHEED-ESC
Contract: 68-03-3249
Lab Code:	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 4.9 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:	SDG No.:
Lab Sample ID: 9S189
Lab File ID: 	
Date Received: 7-23-89
		Date Extracted: 8-1-89
SONC	Date Analyzed:
Dilution Factor:	10
CONCENTRATION UNITS:
uq/kg	Q
319-84-6	
319-85-7	
319-36-8	
53-89-9	
76-44-3	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9	
72-54-8	
1031-07-8	
53494-70-5	
5103-71-9	
5103-74-2	
3001-35-2	
12674-11-2	
11104-28-2	
11141-16-5	
53469-21-9	
12672-29-6	
11097-69-1	
11096-82-3	
aloha-BHC		168	U
beta-BHC		168	U
del ta-BHC		168	U
gamma-BHC (Lindane)		168	U
Heptachlor				168	U
Aldrin		168	U
Heptachlor epoxide		168	U
En dosu 1 -f an I		168	U
Dieldrin-		336	U
4,4' -DDE		336	U
Endrin		336	U
Endosul-fan II		336	U
4,4'-DDD		336	U
Endosul-fan sulfate		336	U
4,4' -DDT		...36	U
Methoxychlor		1682	U
Endrin ketone		336	U
alpha-Chlor dane		163	U
gamma-Chlordane		168	U
Toxaphene		3365	U
Aroclor-1016		1682	U
Aroc lor—1221		1682	U
Aroc lor-1232		1682	U
Aroc lor-1242	 1682	U
Aroc lor-1248	 1682	U
Aroclor-1234	 3365	U
Aroc 1 or-1260—	 3365	U
FORM 1 PEST
1/87 Rev.
occI

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface # :
AutoSampler :
Rack/Vial :
M51Q
9S189
Time
Study
8/31/89 3:55 PM
MCFARLAND
2	Channel ; 1 A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
2:46 PM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e:\pkd\MCFR033.raw
e:\pkd\MCFR0 3 3.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 UL
1.0000 UL
Area Reject
; 0.00
* ## * * EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat flat	Ceapo&wt	Adjuatad Amount Rait Amount P«ak Area Faak Be MULTXfLISt
(mini	Hum	UC/fA	QCltS* (uV-i.e) [uV] AdJfSUu
S.*0 MiDMW
.? »7 mnat
a tt srooi
11.11 BiSfcBIWt
o i at
imia


i,3i	ttiiiBi.oa ¦ lain m
. ¦>» 8TS*e.8g 11 t8»8,8»
>3.83
M' lf ' 71 111
a. a a
Ti , 7Qui

¦ lK

¦vC
M.ta iimoa
l*r» 00*	
ta.>a ehbalp	

rM<
aoTf"»"! o»"
	Q7i»t
U.*0
a__ii2A_U-
0"i>8
•M*-

OO.

25.57 0BC
127.78
182.3*
2.43«6 56084.»»
0.76
Total Arc* - 7»30*#2.00
Total Coacaatraclaa " 1*3.MAS
Report by Tim Rand, Lockheed-ESC
sssssssssrsss
000116

-------
Chroraatoqrara
FileUaae : e:\pkd\KCFR033.rau	Date: 8/31/89 3:55 PN Page 1 of 1	3
Start Tiae: 0.00 ain End Tiat: 47.00 ain Lou Point: -1247457 uV High Point: 2052270 uV
Vertical Scale Factor: 0.00 Plot OffMt: 0 aV Plot Scale: 250 aAr
250.000-
tsj i—i	i*-» KJ
(A «— OO
f-S	I—¦ cjrl d
ro	m	cn	o
H~>	IT)	-a"	*—
^	r-J	cH	—*
—	-—	-—	CN
208.333-
166.667-

cz
CD
CO
a>
125.000-
83.333-
o
o
c
41.667-
-0.000-
-rTTuW'VTT

I	I I
^ s 2
S g fcc1
i i i r3!
i i i'

ss
Lf I *pl
i i i r
-P^T
I I I I I
,-C^l
i i n ¦
7.83	15.67	23.50
Time (niin)
31.33	39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : MS10
Sample Number: 9S189
Operator :
Time
Study
8/31/89 4:22 PH
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : o.oo min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
2:46 PM
Rav Data File
Result File
instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e:\pkd\MCFR03 3.raw
e:\pkd\MCFR033B.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat tiarn Csapenaat	Adjtutad Amount Raw mount Paalt	?aak Bt HUITMLXER
lata)	Nana	UC/Kb	[uV-tmcl [uV] Adj/Raw
i. aft MJUlll	
i.tn onbD
-------
Chromatogram
FlleNaaw : e:\pkd\MCFR033.raw	Date: 8/31/89 4:22 PH Page 1 of 1
Start Tine: 0.00 Bin End Tine: 47.00 "In Lou Point: -1247457 uV High Point: 2052270 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 itt Plot Scale: 250 mV
250.000-
208.333-
166.667-
, S? £5 !£? 63	~ § C=j
^ «iS K cn o	-«r	rv cp — Mi «S
rsj	cn rg

«C
% /
H
o
o
o
Of
£
o
n
en

125.000-
83.333-
41.667-
-0.000-
T VT TT TTTfTrrf

hi
CD
I
o
V a & 8
t-r>
S
St*
i i nfi i i i j~r i it i i*t i r~j i i i i i i 7—1 i j i it i i i i i i | i i i i i i i i i [ i i i i i i i i i
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
41.21 CNDflLD	t-r-94	2606.77	194. .32	
16.09 DDT	571 96—05242. 13	7547.20	54.23 #
55.64 MCTHOXY			2839.75	199.05	
61.41 DBC	192.39 264312.09 23152.77 274.85
: Qoi
4.23
Total Area = 376523.91
Total Concentration = 245.2377
Report by Doherty Bresnahan
000121

-------
FilaNiaa : C:\2700\6CSVCFS031.rw	Data' 8/30/89 7:39 AH Pap 1 of 1
Start Tiati 0.00 tin End Tiaat 70.00 ain Low Point: 3232 uV High Point' 32086 uV
Vertical Seals Factor' 0.00 Plot Offset' 0 nV Plat Scale' 100 aV
Chrotatograa
ltl
* c. s
» »* Si
3
um_l
3
iW-4
5$ ssst; s; ?«*
RiCEKflU**llfcM5 JC ? S aF8 p 118 1IM
I
—m—jsni: iiiiiiirinfrmrtW^Trrr^nrirbr rTrrmnfnrmTi'rf'rTf!! ranrri
t I | I s i a i 6
A	* ? , \ %r 1», 3 S	L
Mt
11.W	a S3	35.00
Tia* (ain)
n.a
S.3J
000122

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : MS10
Sample Number! 9S109
Operator	:
Time
Studv
3/30/89 8s 59 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range s 1000
Data Acquisition Time: 8/29/89 10:26 PM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Samp 1e File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC3\MCF3031. raw
C:\2700\GC5\MCFS031A.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCFS4B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.70
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T emperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400-*5"
.25MM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
15 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 72
**********
EXTERNAL STANDARD REPORT
o.O't -f;
0 i 20 JJ
)d
Ret Time Component Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin]	Name	ug\ !
-------
¦7b. BO EMPESUI
LLA,
U-Z.
40.35 DDD
1.79
2701
¦ r *.<
1 ?t? r»-i
256.39
SJ
i
44.67 EMOOSULFftTE
-0.47
7<=> 79
5(1, 78 ENOK FTQ
-0-.
306.00
18.27


61.41 DBC
244.42 264312.09 23152.77
349.17
Total Area = 628741.50
Total Concentration = 333.2749
Report by Doherty Bresnahan
000124

-------
FileNue : C:\2700\SC3VCF3031.r«	Data: 8/30/89 9:00 AH Pap 1 of 1
Start Tioat 0.00 tin End Tioat 70.00 tin Ion Point: 5232 uV Hi
-------
ID
PESTICIDE ORGAN ICS ANALYSIS DATA SHtET
Lab Names LOCKHEED—ESC Contracts 68—03—3249
£PA SAMPLE NO.
MI 16
Lab Codes	 Case No. s
Matrixs (soil/water) SOIL
Sample wt/vols 30 grams
Levels (low/med) LOW
V. Moistures not dec. 0.2 dec.
Extract ion s (SepF/Cont/Sonc)
GPC Cleanups (Y/N) Y pHs
CAS NO.
COMPOUND
SAS No. s	SDG No. s
Lab Sample IDs 9S195
Lab File IDs 	
Date Received! 7-25-89
		Date Extracted! 8-1-99
50NC	Date Analvseds	:"i
Dilution Factors	10
C CNCEN I"PAT I CM UN IT3:
ka	0
319-84—6	
319-85-7	
319-86-8	
5S-89-9	
76-44-8	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
33213-65-9	
72-54-8	
1031-07-8	
50-29-3	
72-43-5	
53494-70-5	
5103-71-9	
5103-74-2	
8001-35-2	
12674-11-2	
11104-28-2	
11141-16-5	
53469-21-9	
12672-29-6	
11097-69-1	
11096-82-5	
-alPha-BHC	
-beta-BHC	
-delta-BHC	
-gamma-BHC (Lindane)	
-Hep tach 1 or	
-A 1 dr in-	
-Heptachlor epoxide	
-Endosul-fan I	
-Dieldr in		
-4,4'-DDE	
-Endrin	
-tndosu. 1 tan I I	
¦4.4'-DDD	
-Endosul fan suit*ate	
-4.4'-DDT	
-Methoxych lot	 1
-Endrin ketone	
-alpha-Chlordane	
-gamma-Ch1or dane	
-Toxaphene	 3
-Aroc lor-1016	 1
-Aroc lor-1221	 1
-Aroc lor-1232	 1
-Aroc lor-1242	 1
-Aroc lor-1248	 1
-Aroc 1 Gr- 1254	 3
-Aroclcr-1260	 3
160
160
160
160
160
160
160
1 oO
321
321
321
321
321
603
321
160
160
206
603
603
603
603
603
206
206
U
u
u
u
L)
U
U
U
u
u
I I
u
u
u
u
u
u
u
u
u
u
u
u
FORM 1 PEST
Z-CGiJU*
1/87 Rev.

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : N116
Sample Number: 9S195
operator :
Time
Study
8/31/89 4:09 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	¦ Channel : S A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
8:46 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR04 0.raw
e:\pkd\MCFR040.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 0.00
~~~~~EXTERNAL STANDARD REPORT"^
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
Iain!
Coapaaa&e
Adjuatad Mount Saw Amount PaaJt Araa
!uV""e>
Paak Be MULTIPLIER
(uV) A4)ffUw
onrnpow
¦»,m Etmoi
4
is it iima
-t>isa dm	

23.5* DBC
t.li
aa.i*
¦a.n tvit.6*
3>6». *9
»8i6I OlOOOO.gB—1i>6*
191.11
i»"i so-
ui. ua i.2B»g 1JJJ8/.W
n.J« Jiana.aa maau.ft
!!»¦¦»•	
	Wt-
n»ia»
e.asag na*«
-»rW—	1101 ¦ a*
128.as
192.01
2.Stmt S690i.20

j . o i
""T rwr
0.6T-
o.tJ

-ic
-Mt-
Total Araa - 9918290.00
Total Coneaatratloa • *17.k90S
Report by Tim Rand, Lockheed-ESC
CCO!'^

-------
Mil Mite
250.000-
S K SBf^PS b=5 ^ £?;s & JS
~H	>o	CP C> cJ TT	r—.* ct*	^-' «r-l >-} wS
C—I CN t»
208.333-
166.667-

cn

Cki
125.000-
83.333-
41.667-
-0.000-
-nrr^!
r^ri
i T* i fn i i i f-f i Ft T11 i i i i | i i "r* r*f i i i i | i » i i i i i i i | i i i i i i i i i
7 .83
15.67
39. 17
23.50
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : N116
Sample Number: 9S195
Operator :
Time
Study
8/31/89 4:35 PM
MCFARLAND
interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
8:46 FM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
e:\pkd\MCFR040.raw
e:\pkd\MCFR04 0A.rst
e:\pkd\pkd. ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRIUD.seq
2 uL
1.0000 UL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
ssaasssssssssssssss
Rtt turn Ceopaatac	Adjusted teowc Rav Aoouac P««k Aril ?««k He MULXXFLXSL
[nla]	Hum	UC/^ [uV-a«o| [uV] AdJ/IUv


















































-V
23.36 DSC
lit.
VK
133. n
129.*2
2.SS.6 36906.20
0,6?
Total Ana - 7S37«S1.00
Total Concentration • 3*J.*7*3
Report by Tim Rand, Lockheed-ESC
OCO(2Ci

-------
, „ '	Chromatogram
FileMaae : e:\pkd\MCFRMO.rau Date: B/J1/B9 4:16 PH	Page 1 of 1 ^
Start Tine: 0.00 ain End liae: 47.00 nin Lou Point: -1541917 uV	High Point: 2069250 uV
Vertical Scale Factor: 0.00 Plot Offaet: 0 nW Plot Scale: 250 
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : N116
Sample Number: 9S195
Operator	:
T ime
Study
8/30/89 3J 21 AM
MCFARLAND
Inter-face # : 5
AutoSampler : None
Rack/Vial : 0/0
Channel
attached
A/D mV Range : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
I n j. v'o 1 ume
Sample Amount
T ime»
0.00
70.00
1.0
8/30/89
min.
min.
pts/sec
7:06 AM
C:\2700\GC5\MCF503S.raw
C:\2700\GC5\MCF3038.rst
C:\2700\GC5\F0E.ins
C:\2700\QC5\EXSTD.pre
C:\2700\GCS\MCFS1A.smp
C:\2700\GC3\MCF34A.seq
2 uL
1.0000 UG/kg
Area Reject
: 0.00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
0.67
0.00
Bunch Factor:
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sp1i t Rat io
T emperatare
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 13 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 90
it *********
EXTERNAL STANDARD REPORT
Ret Time
[ min 3
Component
Name
Adjusted Amount Peak Area
ug\^>	EuV-sec]
Peak Ht
CuV3
Raw Amoun t
uq\L
30.13 CND01
33.09 D ID-DP IN
~a.a0 SMD03	
12.313 G-BHG	
"M ALDPTN
	0.-42-
—3555.00	
"r23 '~w">
—-533»63
	0 i63 t
•"¦a i
2 HEPEPOX	
	0. 21
	359.99	
	50.15	
0.31
-4-rSS		337,. 91
9.61	20395. 00 1472. 63-

635 y-55~
COC i 3
1/



-------
401 80
ENDrtLD	
	1 Q1OO
22575.75

	2 3. 9'i)
-SS.S7
METHQXY	
	1.39
¦ 'J3
	2363.00
	117.17	
	»t-44
61.40 DBC	166.62 239149.00 21711.74	248.68
I
f
Total Area = 553647.13
Total Concentration = 308.1285
Report by Doherty Bresnahan
-aeetw—
L CC I y —

-------
FileNaaa : C:\2700\GCS\t1CF5038.rM	Data* 8/30/89 8:22 AH Pas* 1 of 1
Start Tiw< 0.00 ain End TiM> 70.00 nin Low Point: S242 uV High Paint: 67740 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 nV Plat Seals: 100
Chmatograx
INI
ft & gg.aSSS ffSSlS X. SSSSfiXfC 33*	3 = «5
3 *9 555? ::&2 k cftansKAit	a aiBb
I i I f I M
11.(7	23.33	35.00
Tin (lin)
53.33
-009^
C CO iB-S

-------
Nelson Analytical 2700 Chromatography System Report Header

Sample Name : N116
Sample Numbers 9S195
Operator	:
Time
Study
8/30/39 9:16 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/0 mV Range : 1000
Data Acquisition Times 8/30/89 7:06 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
I ri ,i. v'o 1 ume
Sample Amount
0.00
70. 00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5038. raw
C:\2700\GC5\MCF5038A.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 US/kq
Area Reject
J 0.00
Noiss Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
0.67
0.00
Bunch Factor:
Instrument Conditions
Capillary GC -
I nstrument
Column
Column Length
Carrier Gas
Flow Rate
So 1 it Rat io
temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400-5
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
160 1/MIN TO 230
200
300
13
Total Number of Peaks Detected? 90
Ret Time
[ m i n J
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
u<3	C uV-sec D
Peak Ht
CuV]
Raw Amount
uq\L
75 A DI1C
-S3 B-BHG
1' '1.56 D-3HC
it. 30 ftLDRIN-
-o ,11 r-pmi naiMF
30.99 A-CHLDAME
Q. 07
15?.61

i555.00-
0. 44	25-75.92
O'J
-176.10
-50.56
	5-55. 00	
0. 66	3343^59	272. 77
0. 75
COO 13^
-ZQ&y-.-22-
-£03. 00
^ o£-
0. 08
0. ?'?
¦1. ts
I

-------
•M.57 OPS	OS. b 377570.00—.2126. 00
¦
V*1
= (\
EMQR uL .. . 		
.. -S-LQ.
-> 7i
- 6664.-63
nr ->g
. -421-
.38
7
-^i|


c-Kinnei n SAtff
1 69
:1595 rt2
29^
96




ENDK€T0	
	9. 42

114.3.
r-±S	
	1r4.
r£<®.

61.40 DBC	211.67 239149.00 21711.74	313.93
Total Area = 669772.73
Total Concentration — 324.5028
Report by Doherty Bresnahan
3^
JOO
Ceo 13 S"~

-------
FileNut : C:\2700\GC3\rtJ5038.rat.	Dats: 9/30/89 9:17 AH Pag* 1 of 1
Start Tin! 0.00 ain End Tinas 70.00 ain Low Point: 5242 uV High Point: 67940 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 «V Plot Seals' 100 aV
Chraaatograi
INI
k k (| !• SS5 8 C 8 !| 8 J •!33SIS" 3S! % ISSR^ 9-}!|
- 3 +2S2Z 5 SsRX R CSxtlAMPill 555 CSSlB f<* fife* 8 828ft
|
II
n
5
1(1X7-3
11.W	23.33	35.00	H.U	58.33
TiM (ain)
-QWISOon
ocorit.

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
t£PA SAMPLE NO.
OFOl F'REGPC
Lab Name: LQCKHEED-ESC
Contract: 63-03-3249
Lab Cade: 	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
Moisture: not dec. 1.9 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) N pH:
CAS NO.
COMPOUND
SAS No. : — SDG No. s
Lab Sample ID: 9S177
Lab File ID: 	
Date Received: 7-25-89
		Date Extracted: 7-31-89
SONC	Date Analysed: &'3C'%"ci
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-34-6	alpha-BHC		32	U
319-35-7	beta-BHC			32	U
319-36-3		del ta-BHC		32	U
58-89-9	qamma-BHC (Lindane*		32	U
76-44-8	Heptachlor				32	U
309-00-2	Aldrin		—	82	U
1024-57-3	Heptachlor epoxide		92	U
959-98-8	Endosu 1 fan I		32	U
60-57-1	Dieldrin		163	U
72-55-9	4, 4'-DDE		163	U
72-20-8	Endrin		163	U
33213-65-9	Endosu 1 fan II		163	U
72-54-8	4,4' -DDD		163	U
1031-07-8	Endosulfan sulfate		163	U
50-29-3	4, 4'-DDT		icZ	U
72-43-5	Methoxychlot		315	LI
5-494-70-5	Endrin ketone			1j3	'J
5103-71-9	alpha-Ch lor dane		32	U
5103-74-2	gamma-Ch lor dane		32	U
3001-35-2	Toxapnene		o 31	U
12674-11-2	Aroclor-1016				315	U
11104-28-2	Aroc lor-1221	'		315	U
11141-16-5	Aroclor-1232		315	U
53469-21-9	Aroc lor-1242		315	U
12672-29-6	Aroc lor-1248		815	U
11097-69-1	Aroc lor-1254		1631	U
11096-82-5	Aroc lor-1260		1631	U
FORM 1 PEST	1/37 Rev.


-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : OFOl Pre-GPC
Sample Number: 9S177
Operator :
Time
Study
8/30/89 1:36 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
4:14 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 2 2.raw
e:\pkd\MCFR0 2 2.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 UL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rae Tin
total
Coopooanc
Adjuacad /Amounc Raw Amount Paak Araa Paak Be MULTIPLIER
UG	UC/L [uV-i«c| (uV]	Adj/Raw
iittchlh
ALDRIW	
-iS.SS-£WK»	
47.«» BBt	
25.73 DBC
a. tii
1 mi6(i rm	'¦««¦» •»«
—13900 ¦ 00
73. W -
0.*8	
107.4 3
	9^4-
19810.75
013.90
saa.t?
27.07
137.29
39.oa a>9*sa.aa oaa».7*
201.90
2.69a« 61822.AO
-9t-68-
. <*»
. f.v»
a.jg
0.00
3.68
Total Araa • 5*12498.00
Total Coocantcatian » 238.9328
Report by Tim Rand, Lockheed-ESC
jQQQ122-&3
qOO(3?

-------
Chromatog ram
FileNaae : e:\pfcd\HCFR022.raw	Date: 8/30/S9 1:36 PH Page 1 of 1
Start Tine: 0.00 ain End Tiao: 47.00 as in Low Point: 4700 uV High Point: 70*890 uV
Vertical Scale Factor: 0.00 Plot OfUet: 0 bW Plot Scale: 250 atl
250.000	
208.313
166.667
125.000	
CO

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number:
Operator
Interface #
AutoSampler
Rack/Vial
OFOl Pre-GPC
9S177
Time
Study
8/30/89 2:24 PM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
4:14 AM
Raw Data File :
Result File
Instrument File:
Process File
Sample File :
Sequence File
Inj. Volume
Sample Amount :
e:\pkd\MCFR022.raw
e:\pkd\MCFR0 2 2A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Rat Tlaa
[mini
Caopeaaac
Adjtucad Amount Raw Amount P«*k Ax*> Pafck He MULTIPLIER
».«» B BH0
i.tg ALD1UM
0»:65~
UC/L
(uV-««c)
[uV]
AdJ/Raw
-UK"
ODfl
-13.63 ODD
25.73 DBC
—o.3a—
	on—
-frrW—20960.00 1368.89
0.36-
-0.26 5390,00	350.15-
17
- -O-HW-
23.1fr-
164.04
110.

- 1.20 10010.73
33.96 906136.06
241.23
320.6?
5163.30
2.69«6 61822.60
0. 00
: ^
i ^
0.60
0.60
-Or^fl	t^iS
0.68
Total Ar«& • 5383488.00
Total Concentration • 268.3824
Report by Tim Rand, Lockheed-ESC
oooiaa-^a
CQO110

-------
Chromatogram
FileNaoe : e:\pkd\HCFR022.raw	Date: 8/30/89 2:24 PM Page 1 of 1
Start lias: 0.00 ain End Tiae: 47.00 ain Low Point: 4700 uV High Point: 704890 tN
Vertical Scale Factor: 0.00 plot Offset: 0 oV Plot Scale: 2S0 mV

c=
o
cd.
CO
«X»
o
o
c
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
—4 o CTt
2 ^ ^
2
U-> Cm
li> CO
iri r~»*
CM

Vnr.T
»—rrr
• -|

c_> o
o
I
it S
LO
S

i *Pi i i i i i*? i i*Y i Fj i i i i i i T*1! i | i i? i i i i i i j i i i i i i i i i j i i i i i i i i
7 . 83
15. 67
23 . 50
Time (min)
31.33
39. 17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
Inter-face #
AutoSampier
Rack/Via j.
OFOl pre-gpc
9S177
5	Channel
None attached
O/O
Time
Study
8/29/89 10:14 AM
MCFARLAND
A/D mV Ranqe : 1000
Data Acquisition Time« 8/29/89 7:37 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
0. 00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5015E. raw
C:\2700\GC5\MCF5015G. rst
C:\2700\GC5\F0E.ins
C:\270O\GC5\EXSTD. pre
C:\2700\GCS\MCF51A.smp
C:\2700\GC5\MCF54A. seq
In .j,
Volume
Sample Amount
Noise Thresnold
Dilution Factor
Divisor
2 uL
1.0000 US/kg
1
1.00
1.0000
Area Re-sen	• 0.00
Area Thresnold : 100
Mul t ip 1 ier	:' 0. 63
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow n-i.ts
Split Ratio
T SiTparaturs
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400—5"
.25MM ID .25UMFILM RTXS
30M
HE
20CM/SEC LINEAR VEL0CIT
160 1/MIN TO 230
200
300
15 PS I
Total Number o-f Peaks Detected: 42
Ret Time
Cmin 3
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount
ug-vC c

Peak Are*
CuV-sec 3
Peak Ht
CuV3
Raw Amoun t
ua \L
10. *75 HPTC1ILR
-ts-
437.00
604'?. 00
o. n3
1.4h
I
-a-1.25 ALDHlIH
27.05 IICPEPQX
9iLi
17
-3S-
320.42
712-.0O	5-2-.-9S-
1342. 50	T~ ~
30.10 ENPQ1
33.93 DIELDHIN
30.15 CN001
80S.00
i.... j
5S. a4
-•>-.-23-
7 64.00
52. o:
000131-t^
OCOI*^
0.01
. 4

-------
—40. 73 ENDALD	-	S*-£S	2859.00	261.02	3.01 *^
16.00 DDT 				—37*75757	ZS557ST"	SO.aa ^
554 04 HCTI IOXY	3t4«	1846.00	115.91	5-g	00- **
61.33 DBC	164.. 10 232072.00 18086.73 241.32
Total Area => 279346. 19
Total Concentration = 185.8399
saaaasaasssssssasssaaaaaaaassasssssBsssessssaasssaasssass
Report by Doherty Bresnahan
QQ0132
6^-6 ' *-/ i

-------
FileNua : C:\2700\SC3\nCF301SE.rati	Data: 8/29/89 10:13 All Pa« 1 of 1
Start Tiatt 0.00 ain End Tiati 70.00 ain Low Point: 51*4 uV High Point: 28034 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
ChroMtogTU
sag* 53 9SS53*S8S Sis?9 * g t s )i ^ ; S
- >< 3k jss u xaa b n*in: 3 : 0 tc u i 1
I
u
It
s
3
15557-3
1 ik
3-iV-rr*-
t»41
i
i I
i—L
II illlll
u
iiiiili n 11 iiaiii'im
s *
» ¦
.t 1 w
1U7

a.® n.a
Tii* (aia)
58.3
000133
ccom

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : OFOl
Sample Numbers 9S177
Operator	:
T ime
Study
8/29/89 2:09 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time* 8/29/89 7:37 AM
Delay Tims
End Time
Sampling Rate
0. 00
70.00
1.0
min.
min.
pts/sec
Raw Data File
Result File
C:\2700\GC5\MCF5015E. raw
C:\2700\GC5\MCF5015K. rst
Instrument File: C:\2700\GC5\F0E.ins
Process File
Sample File
Sequence File
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
In.i. Volume
Sample Amount
2 uL
1.0000 UG/kg
Area Reject
: 0. 00
Noise Threshold
Dilution Factor
Divisor
I
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
too
0.68
0. 00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
3p 1 i t Rat io
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 42
Ret Time
Cmin ]
**********
Component
Name
EXTERNAL STANDARD REPORT
-t-l .-56 B-BHC
13.60 D 01IC ¦ ¦
11.25 ALDRIN
Adjusted Amount Peak Area
UW IL
£/
-rr
•> -%-f ¦
CuV-sec]
Peak Ht
CuV]
Raw Amount
ug\L
040.50
2t
1052.99-
68.94
30.99
0.54
¦ t/H
. l.*l
O.13—
1.50-
-l-r*2	6049. 00
-*>r09-
320.42
20.94 0 CIILDANC
30.92 A CIILDANC
^-29. 00
700.00
42.60
60.67
0. 16
63.77 237230.00	22390.17
— {.4S
JO
0. 23
r4.Cil DDE
eeottrr"©
OOC 1-f S"
Vb.

-------
•361 06
CNDniN	

0 ¦ So
6Q6i WJ
	6oi64
in
0. 70
a n-r
.it a a









1 A

< /I Crt -r 4
. e- f
61.38
DBC

208.48
232072.00
18086.73
306.58
Total Area = 546144.50
Total Concentration = 287.5825
Report by Doherty Bresnahan
eeetaso-i
CCO I Y6-

-------
FileNua ' C:\2700\GC5\flCF5012E.ru	Oat»: 8/29/89 2:10 PH Pag* 1 oi 1
Start Tioai 0.00 ain End Tim 70.00 ain Loh Point: 5144 uV High Point: 3)034 uV
Vertical Seals Factor: 0.00 Plat Offset: 0 aV Plat Scale: 100 uV
ChxoBatograa
,	• «•«**>» * Jj 3
x b ua a nmnvz s
i
u
I
tt
41
is.w-3
LA
ta|_ti'T7n—mr
111?	23.33	33.00	5iB
TiM (tin)
COO I ^'r-

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
0802
Lab Name: LQCKHEED-ESC
Contract: 68-03-3249
Lab Code:	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 4.9 dec. 	
Extraction: (SepF/Cont/Sonc) SQNC
GF'C Cleanup:  Y pH:
CAS NO.
COMPOUND
SAS No.:	3DG No.:
Lab Sample ID: 9S178
Lab File ID: 	
Date Received: 7-23-89
Date Extracted: 7-31-89
Date Analyzed:
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	
319-85-7	
319-86-8	
76-44-8	
309-00-2	
1024-57-3—
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9-
72-54-8	
1031-07-8—
"2-43-5	
53494-70-5-
5103-71-9—
5103-74-2—
3001-35-2—
12674-11-2-
11104-28-2-
11141-16-5-
53469-21-9-
12672-29-6-
11097-69-1-
11096-82-5-
a 1pha-BHC		168
beta-BHC		163
delta-BHC		163
gamma-BHC (Lindane)		163
Hep tach 1 or		163
A1 dr in		168
Hep tach lor epoxide		168
Endosul -fan I		168
D ie 1 dr in		536
4, 4' -DDE		336
Endrin		-536
Endosul-fan II		336
4, 4'-ODD		•-"•36
¦Endosul fan sulfate		336
"i,4'-DDT		.'36
'f1etho:;ycn lor—		—	1=32
Endrin ketone		--36
•alpha-Ch lor dane		168
•gamma-Chlordane		168
¦Toxaphene		3365
Aroclor-1016		1682
¦Aroc lor-1221		1682
•Aroc lor-1232		1632
¦Aroc lor—1242		1682
¦Aroc lor-1248		1632
¦Aroc lor-1254		3365
¦Aroc lor-1260		J365
U
U
U
U
u
u
u
IJ
u
IJ
u
u
u
u
u
u
IJ
u
u
u
u
u
u
FORM 1 PEST
1/87 Rev.
cco f4£

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface #
AutoSampler
Rack/Vial
0802
9S178
Time
Study
8/30/89 1:46 PM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
5:58 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR024.raw
e:\pkd\MCFR0 2 4.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
R«e Tlo* Co^eMst
Coin] Ksm
Adjuatad Amount Raw Amount
UC/L UG/L
Peak Ar«a
(uV-i«c|
Paak Be
tu»]
MULTIPLIER
Adj/Raw














25.66.0BC
100.S3
1*4.0*
1.92a6
*4141.24
0.70
V/-
Total Aria - 3298281.00
Total Concentration " 134.9016
Report by Tim Rand, Lockheed-ESC
0COW

-------
FileNaoe : e:\pfcd\MCFR024.raw	Date: 8/30/89 1:46 PM Page 1 of 1
Start Tlae: 0.00 ain End Mae: 47.00 ain Lou Point: -1810287 uV High Point: 669870 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale; 250 cnV
250.000
208.333
166.667	
125.000
CO

Ck£
83.333
O
O
O
( 2*1.667
-0.000
3


-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number:
Operator
Interface #
AutoSampler
Rack/Vial
0802
9S178
Time
Study
8/30/89 2:27 PM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
5:58 AM
Rav Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR02 4.raw
e:\pkd\MCFR024A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rac Tim*
(Bin]
Coapoatat
>>¦«» BBB
u.ta DiiBaaumnB
25>66 DBC
Adjuacad Amount Raw Amount Paak Araa
UC/L	UG/L [uV-aac]
Paak Ht
tuV]
MULTIPLIER
AdJ/Raw
-Trr~



¦ lo.ia



63



or

laise





rtl

13 ill
120.47
11.19 1IIIH.M iW.M
172.10 1.92a6 44143.24
8. >»
0.70
%-


Total Araa • 3896*37.00
Total Concentration - 198.333*
Report by Tim Rand, Lockheed-ESC

000140
CCOISI

-------
Chromatoqram
FlleUaae : e:\pkd\MCFR024.rau	Date: 8/30/89 2:27 PH Page 1 of 1	7
Start liae: 0.00 ain End Itae: 47.00 ain Lou Point: -1810287 titf High Point: 669870 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 250 nV
Oj
CO

Oct
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
.000-
ro o o ki p^.
2 3 S93 5 5 S
• •	• • i
O	CD
•— V »£»
cn os rs
An.^n^r-r^
' I	I
i i 1*1 *r\ i i i |T i inr i i Fj i i i i i i T*i r i i i^P i i i i i i | i i i i i i
i • ¦
7.83
15.67
23 . 50
39. 17

-------
		Nelson Analytical 2700 Chromatography System Report Header
Sample Name : 0802
Sample Number: 9S17S
Operator	:
Time
Study
a/29/89 12:01 F'M
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Ranqe : 1000
Data Acquisition Timet 8/29/89 10<05 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5022.raw
C:\2700\GC3\MCF3022.rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
Inj. Volume :	2 uL
Sample Amount :	1.0000
Noise Threshold:	1
Dilution Factor:	1.00'
D i v i sor	•'	1. 0000
UG/kg
Area Reject	: 0.00
Area Threshold '• 100
Multiplier	: 0.70
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
T emperature
Injection Teinp.
Detector 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
F S I
160
200
300
1/MIN TO 230
Total Number a-f Peaks Detected: 43
EXTERNAL STANDARD REPORT
»***
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin]	Name	ug\L	CuV-sec] CuV]	ug\L
12. 1" G-BHC		<186.50 64.23	OjI-W^
>21.25 ALDRIN	0. 37	2274 . 00	145.60	0.5"
'26.17 HEPEFOX		6236. 00	332. 42	2.22
29. ^ CNDQ1	7.21	27169.50 2000¦ 65	10.30
33.53 0 ID-DP IN				1--3B-—-2793.00 262.63	1. 76 iM
¦=0.26 CND02	0. 50	1627.04	00.01	
000142^
COO / S3

-------
I
,1 £5*
CMDALD	
	11.75..
1579a,61
—1-30.3.6?	
161 7 6




4 -re
i fn < 1
w w 1 ^ U
61.33
DBC
125•£>3
172594.00
1.2343.98
179.47
Total Area = 248132.13
Total Concentration = 139.5630
Report by Doherty Bresnahan

_0©(H43^
Ceo i ^

-------
Fileftw : C:\2700\EC3\MCF3022. r»	Data: 8/29/89 12:02 PH Pi;* 1 of 1
Start Tiaai 0.00 ain End Timi 70.00 ain Ion Point: 5061 uV High Point: 411299 uV
Vertical Seal* Factor: 0.00 Plat 0«*t: 0 «V Plot Scala: 100 aV
Chroutogru
5
u
41
Ql
UWH
tun—=
sw-j
5WH
II.®-:

34-=
'nrr
% ?	s ? ft =5 ts
B S iGII&KaRMM; :: !!R I t li i I
mrniMiiifoniirttia mfii mil 11 w a nfm
i 1 § 1 11
& i i f, i i r. . Y. ¦ it i r.
JLjl
1LW	8,8	3.00
Til* (tin)
58.33
ooo IS^~

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : 0802
Sample Numbers 9S173
Operator	:
Time
Studv
8/29/89 2:23 F'M
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attacned
0/0
A/D mV Ranqe : 1000
Data Acquisition Times 8/29/89 10:05 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument Fil<
Process File
Sample File
Sequence File
0.00
70.00
1.0
mm.
m in.
pts/sec
C!\2700\GC5\MCF5022.raw
C:\2700\GC5\MCF5022A.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GCS\MCF51B. smp
C:\2700\GC5\MCF54B. seq
Inj. Volume
5 amp 1e Amoun t
2 uL
1.0000 UG/kq
Area Reject
: 0.00
Noise Threshold
Dilution Factor
Divi sor
t
1. 00
1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
0. 70
0. 00
Buncn Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
'2c 1 i t Ratio
Temperature
I n .1 ec t i on T ernp
Detector 1
Detector 2
Notes
VARIAN 3400-5"
.25MM ID .23UMFILM RTX3
30M
HE
20CM/SEC LINEAR VELOCITY 13 PS I
160 1/MIN TO 230
2(30
300
Total Number o-f Peaks Detected! 49
EXTERNAL STANDARD REPORT
Ret Time
Cminl
Component
Name
Adjusted Amount Peak Area Peak Ht Raw Amount
ug\L	CuV-sec] CuV]	ug\L
¦12. 4«>
0 DUG	


	Igfc.Stt
	64.2Z	
	Q. Z I
iA'
1 •

cc
13.10-
AT 1 HS /.T.

1 E


/• /r


•tO ffiC



i/tr.
*7 C L.
¦¦ / / ju i • yu-



36.70
CNDftIN	

	1. 26
	1577.23
	74 . i'*i^	
	1. 90

009*4536
OGGi^
I
II	•
I

-------
40. 26
	
	26.17
596051 56
—2604.06	
	57.59 ?






61 • wO
DBC
159.61
172594.00
13543.98
228.01
Total Area = 393477.44
Total Concentration = 226.0109
Report by Ooherty Bresnahan
Q0Q146 '¦«
6 CO )

-------
FileNaaa : C:\2700\SC3\f1CF3022. rw	Data: 0/29/89 2:23 PM Paw 1 ofl
Start Tiatt 0.00 ain End Tiaes 70.00 ain Low Point: 3061 uV High Point: 411299 uV
Vertical Scala Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Chroiatogra*
5 S RXIK KSRRXM
n.a a a 33.00 #.w a.*
Tia* (ain)
-e6e±4T#>
COO /S?

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
fcFA SAMPLE NO.
P715
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Code:	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
V. Moisture: not dec. 0.7 dec. 	
Extraction: (SepF/Cont/Sonc) SONC
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:———— SDG No.:
Lab Sample ID: 9S194
Lab File ID: 	
Date Received: 7-25-89
Date Extracted: 8-1-89
Date Analyzed: *9'3c-&ci
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	
319-85-7	
319-86-8	
58-89-9	
76-44-8	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9	
72-54-8	
1031-07-8	
53494-70-5	
5103-71-9	
5103-74-2	
8001-35-2	
12674-11-2	
11104-28-2	
11141-16-5	
53469-21-9	
12672-29-6	
11097-69-1	
11096-82-5	
-a lpha-BHC		161	U
-beta-BHC		161	U
-delta-BHC		161	U
-gamma-BHC (Lindane)		161	U
-Heptachloi		161	U
-Aldrin		161	U
-Heptachlor epoxide		161	U
-Endosul -fan I		161	U
-Dieldrin		322	U
-4,4'-DDE		322	U
-Endrin		322	U
-Endosul-fan II		322	U
-4,4'-DDD	:		322	U
-Endosul-fan sul+'ate		322	U
-4.4'-DDT		322	U
-Methoxychlof		1611	'J
-Endrin ketone		322	U
-alpha—Ch lor dan e		161	U
-gamma-Ch 1 or dane		161	U
-Toxaphene		3223	U
-Aroclor-1016		1611	U
-Aroc lor-1221		1611	U
-Aroc lor-1232		1611	U
-Aroc lor-1242		1611	U
-Aroclor-1248		1611	U
-Aroc lor-1254		3223	U
-Aroc lor-1260		3223	U
FORM 1 PEST
1/87 Rev,
oco<±'ci

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface # :
AutoSampler :
Rack/Vial :
P715
9S194
Time
Study
8/31/89 4:07 PM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
7:55 PM
Raw Data File
Result File
Instrument File:
Process File
Sample File
Sequence File
inj. Volume
Sample Amount
e:\pkd\MCFR039.raw
e:\pkd\MCFR0 3 9.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
0.00
~EXTERNAL- STANDARD REPORT*****
Instrument ID: varian 3400-1	GC Column ID: 2250/2401
Rat Tlaa
(mini
AdJujtad Amount Raw Amount Paak Aria Peak He MULTIPLIER
UOltjk.	UC fjtfc [uV-aae) [uV] AdJfRaw
1.1 3i llfiTSBtfl
>1 HCTPO*
q»aa amat
H nmMTB
Hi 89 BIBQ»
ni»> aai
23.33 0BC
lit'
a.aa iaat8i»8
1.08
i.it
a¦ fia	ooaoie
aaa ¦»
Hita
uni.
ta.aa
j.( hi aa
" 134.30
as.
wa.oe
-MM
.ailTBl.i
>>.aa atan.a

200.73
2.67a6 61366.1
r«-
i.ar
3.BT
a.ta
0.61
0.67
—	vt
—i»c
—	UC
¦\»c
—
— v*.
Total Acaa - 12836999.00
Total ConctacrftClon • 515.3456
Report by Tim Rand, Lockheed-ESC
CccIO

-------
Chromatogram
FileNaoe : e:\pkd\MCFR039.raw	Date: 8/31/89 4:07 PH Page 1 of 1
Start Km: 0.00 ain End lias: 47.00 sin Low Point: -1558947 uV High Point: 1927010 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 bW Plot Scale: 250 mV
250.000
208.333
166.667
125.000
13.333
rr~
-0.000
£3
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Sample Name : P715
Sample Number: 9S194
Operator :
Nelson Analytical 2700 Chromatography System Report Header
4:33 PM
Time
Study
8/31/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
7:55 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR039.raw
e:\pkd\MCFR03 9A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
~EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
R«t flat	Coapoamt	Adjusted Aaotmt Raw Aaeusc Peak Ar«« P««k Be MULTIPLIER
(ffllA)	Nam	UC/JCJjfc	UG'f/k (uV-.«c| [uV] Adj/SUv
GfHiPAltD ¦
ift.at m
II 39 PPP
&TF
DirPCCVbTAgB
25.55 0BC
0.0*



ia?i

!» M
369.»9

• a,n mi t\ aa atattia?
aa.a«
160.70
m
239.85 2.67*6
»0
61366.10
8.67
J i <11
-l/K-
-M-
0.6* iS



0.67
Total Arta • 11475921.00
Total Coaeaatratloa ¦ 475.4975
Report by Tim Rand, Lockheed-ESC
CCOI^

-------
Chroroatograra
FileUaae : e:\pkd\HCFR039.rau	Date: 8/31/89 4:33 PM Page 1 of 1	^
Start Tiaes 0.00 ain End Tias: 47.00 ain Low Point: -1558947 uV Nigh Point: 1927010 uV
Vertical Scale factor: 0.00 Plot Offset: 0 «V Plot Scale: 250 oV
u->
m
oO
250.000
208.333
166.667
125.000
41.667
rr
-0.000
CJ
7.83	15.67	23.50	31.33	39.17
Time (rain)

-------
Sample Name
Sample Number
Operator
Inter-face #
AutoSampler
Rack/Vial
Nelson Analytical 2700 Chromatography System Report Header
P713
9S194
5	Channel
None attached
0/0
Time
Study
8/30/89 8:16 AM
MCFARLAND
A/D mV Range
1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
Timet 8/30/89 5:52 AM
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5037.raw
C:\2700\GC3\MCF5037.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Re .1 ec t	: 0. 00
Area Threshold : 100
Multiplier	: 0.67
Additive Constant: 0.00
iunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
5pIi t Ratio
Tamper ature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400-S"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 13 P3I
160
200
300
1/MIN TO 230
Total Number af Peaks Detected: 68
~
Ret Time
C m i n 1
rnttt
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
uq \ .!$a.	 CuV-sec 3
Peak Ht
iuV]
Raw Amount
uq\L
frS.42 (3-BHC
flLBRIN
4 HSP'EPQX
HQ. 2.1 EMD01
53.91 DIELDRIN-
*3,
s.mdo:
-ii.
MM. 23
112.-8
It. 10	90271.50
-a®
. m •
'<7» 1Q
-^=r >$$£.
21.04
- 'jr^H
4-504.50
131.OS
-l-w-OO-
3918.00
137.10
I. -19
Qooisa-^
OGCIW
	3". €*5	o 43^i i 37
		9157.00
500.00
). S3
AIS.67
-4th
f
I

-------

ENDrtLO	
	17.90
2D2Q7.00
	1763.02	
	26. 34*

MCTUnY V
¦? 38
« OTA ,-,/1
19'ltel • 1 J
1 A £. AO

61. 40
DBC
194.44
279087.00
24029.09
290.21
ooi
is>
Total Area = 592509.25
Total Concentration = 311.3402
Report by Doherty Bresnahan
C'C 0

-------
FilaNtM : C:\2700\GCS\MCF5037.rw	Date: 8/30/89 8:16 AN Pag* 1 oi I
Start Tioat 0.00 ain End Tiw* 70.00 nin Lot* Point: 5249 uV Hiah Point: 806661 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 uV
Chromatograi
5
a
U
%
INI
« a *3 s ft* 3*?ca esftS	mc
* 3 • 9 B 5S SZ S KR CffRA * «»« CSJS 7a C R Kl I fi >86
501

I ,
H'H^irnniiiini mil i m i 111iff'rrr^rrrr'rrrnWrrriii; n:: u n' i'! iiiiit
* j i I a I j|
.'I I I ¦ I*. I ?i I I "i I r. I ?l . it I Hi
11.(7
23.33
35.00
Til* (tin)
4U7
58.33
fleeiss*^
coc \L-L-

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P715
Sample Number: 9S194
Operator	:
T ime
Study
8/30/39 9:13 AM
MCFARLAND
Inter-face #
^utoSampler
Rack/Vial
5
None
0/0
Channel
attached
A/D mV Range
1000
Data Acquisition Timet 8/30/89 3:52 AM
Delay Time
End Time
Sampling Rate
3aw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF5037. raw
C:\2700\GC5\MCF5037A.rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C: \2700\GC5\MCF51B.smp
C: \2700\GCS\MCFS4B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.67
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions
Capillary (3C -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Rat io
T smperature
Injection Tamp
Detector 1
Detector 2
Notes
VARIAN 3400 - S"
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
13
= 1
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 68
Ret Time
Cm in 3
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount
u
Peak Area
CuV-sac]
Peak Ht
CuV:
Raw Amoun t
uq\L
l'0. 21 (V-BHG
12. lu D DIIC
D-BHG
1. 40
0. <\2
a 00
602.75
--703rt-4-
i ¦	^
74.34-
-1-4-71 14-
occlb*
2.00
0. '15
0. Q'J
2iXJtt-
6LDRIN	—
n r*i_n aakic
	14.95
^>271,50
2Q37.10	
	22,31
SI. 02
fi 'GHLDANE	
	0. 4 4
77-T An
17" • i
—isx^as	
	0. 64

-------

¦w£	
	=4-Bt
¦££-
-"-i
967130.25
Q16191OQ	
	325.66

DDt>
1 L
00



'1') h T
CMnnci ii catc





g 1 i
EHDKETD

A-y


' • fc w
61. 40
DBC
247.
02
279087.00
24029.09
368.69
i s
Total Area = 1391773.73
Total Concentration = 505.9161

Report by Doherty Bresnahan
Q60t57TPfi
cCulOk

-------
FileNaw : C:\2700\6C5\flCF3037.ran	Date: 8/30/89 9:14 AH Paqe 1 of 1
Start Tiu< 0.00 ain End Tiae> 70.00 ain Low Point: S249 uV High Point: 806661 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mV Plot Scale: 100 aV
Chrctatogra*
I
II
i
9	W 3 «£ S?,?S3 CSfiS SSXStf *63ft*3 bite
2 «J5 J! tZ B RS ERaA X KMH9 C5!! SB P D tin I » 1 Ift
ra
JL±*L
H •
a t - 5 .
V * 3 s , 3
a	*
i i
* i T
nw 23.33 35.00 #.w
Tiw («in)
i1 ¦
58.33
«OOt5«-u.3
C&G

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
tPA SAMPLE MO.
P803
Lab Names LOCKHEED-ESC
Contract: 68-03-3249
Lab Code: 	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/voi: 30 grams
Level: (low/med) LOW
*/. Moisture: not dec. 1.7 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:	—— SDG No.:
Lab Sample IDs 9S179
Lab File ID: 	
Date Received: 7-25-89
		Date Extracted: 7-31-89
SONC	Date Analysed:
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	0
319-34-6	a lpha-BHC	
319-85-7	beta-BHC	
319-86—3	del ta-BHC	
53-89-9	gamma-BHC (Lindane)	
76-44-8	Heptach lor	
309-00-2	A1 dr in	
1024-57-3	Heptachlor epo:;ide	
939-98-8	Endosu 1 -fan I	
60-57-1	Dieldr in	
72-55-9	4, 4' -DDE	
72-20-8	Endrin	
33213-65-9	Endosul-fan II	
72-54-8	4,4'-DDD	
1031-07-8	Endosu 1 -fan sul tate	
72-43—3	Mstho;
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P803
Sample Number: 9S179
Operator
Time
Study
8/30/89 1:49 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition	Time: 8/30/89 6:50 AM
Delay Time	:	0.00 min.
End Time	:	47.00 min.
Sampling Rate :	1.0 pts/sec
Raw Data File :	e:\pkd\MCFR025.raw
Result File :	e:\pkd\MCFR025.rst
Instrument File:	e:\pkd\pkd.ins
Process File :	e:\pkd\pextstd.prc
Sample File :	e:\pkd\clpa.smp
Sequence File :	e:\pkd\MCFRLND.seq
Inj. Volume
Sample Amount
2 uL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT1*
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Rat Tlaa
[min)
Covenant
Adjuatad Afflounc Raw Amount Paak Araa Paak Bt
US/L	UG/L [uV-sac] tuV)
MULTIPLIER
Adj/IUw
%
i ts r.mr
IIBPEPWi
9it» BtBBI
19.89 PIKgaiM
;3. 39
17.68 OPT
H.88 BIIBMJ
23.61 OBC
B.li
i.18 maB.aa
-8.88
r&i-
a.it laam.aa sos9iit
ia.*i
0*i70
u.m »
114.17
~rW

16$. 20
2.24a6 31443.41
a.aa
0.60-
9.66
o.ao
a. ta
8.48
0.68
Total Araa • 8571060.00
Total Concanczatlon ¦ 440.4071
Report by Tim Rand, Lockheed-ESC
aaaaea:
C cO i'^ '

-------
Chroma tioararo
FileNaae : e:\pfcd\HCFR02S.rau	Date: 8/30/89 1:49 PH Page 1 of 1	^
Start Tine: 0.00 ain End Tina: 47.00 ain Low Point: -172SS77 uV High Point: 1959030 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mi Plot Scale: 250 mV
ad
250.000
208.333
125.000
333
PT
-0.000
7.83	IS.67	23.50	31.33	39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P803	Time	: 8/30/89 2:29 PM
Sample Number: 9S179	Study	: MCFARLAND
operator :
Interface #
AutoSampler
Rack/vial
2	Channel : 8 A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
6:50 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	;
Sample Amount	;
e:\pkd\MCFR025.raw
e:\pkd\MCFR025A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
* * * * * EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
sassnsssssss

R«C flSM
Caia]
CoflpocttsM*
Mjuatad Mmnt IUw Amount Nik Art* t*ak He MULTIPLIER
UG It	0C/L	(uv; Adj/Raw
a o Ci.cai.Mm
11	19 t.ffBLBOiiHI
10	»3 ppg	
11	oi Eimatit
¦>l »a BBB
ti.io mnwowjoM
23.61 DSC
rW-
i8.li eg woo. oo ijea?9i
?W"
!.«.b» inaiB.aa lmn.asi
-nr
—»T
w
ua.u
		 0"'p8»
z.snv
10T330.W
—aaa.a*	¦

19.81 HUJBB.lt
59.O |]»>g0i0»
/BSB.it
isori. o-9	
136.63
200.94
2.24*6 31463.41
flrM	\'f-
vrss	
~9
rsv

it-
-it.
0.6S
Total Ar«m ¦ 6401040.00
Total Concentration - 301.8*11
Report by Tim Rand, Lockheed-ESC
sasssssaasss
iCO I'13

-------
Chromatoqram
FileMaae : e:\pkd\MCFR025.raw	Date: 8/30/89 2:29 PH Page 1 of 1	^
Start fiae: 0.00 ain End fiae: 47.00 afn Low Point: -1725577 uV High Point: 1959030 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 uV Plot Scale: 250 raw
250.000
208.333
166.667
12S.00Q
-C
n,
-0.000	
7.83	15.67	23.50	31.33	39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : P803
Sample Number: 9S179
Operator	:
T ime
Study
8/29/89 1:15 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time:
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount :
Noise Thresholds
Dilution Factor:
Divisor	:
0.00
70. 00
1.0
8/29/89
min.
min.
pts/sec
11:20 AM
C:\2700\GC3\MCF5023.raw
C:\2700\GC5\MCF5023.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.68
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capi1lary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Rat i o
T emperature
In j ec t i on Tamp.
Detector 1
Detector 2
Notes
VARIAN 3400 -5"
.25MM ID .25UMFILM RTX3
30M
HE
20CM/SEC LINEAR VELOCITY
15 PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 87
Ret Timt
[min ]
*********
Component
Name
EXTERNAL STANDARD REPORT *********
Adjusted Amount Peak Area Peak Ht
uq\L	CuV-sec] CuV]
Raw Amount
ug\L
10.23 HPTCIiLr<
¦21.36 ALDHIM
-43-
1235.50
9526« 67
914 55
¦>59. 40
r64—

1.99
¦26.20 HEPEP0X
:.00 CND01	
1.93 DICLDniN
-2-.+e-
9000.50
6.60 25096.50
6.20 12966¦3fl
563.44
1955. 14
3. 20
9.02-

347. 93

¦30.22 CNDQ2
jQjQOlb'l ^
c-00 Us
.•} . 40	1 4015. 00
994.56
u . 47—ztf,

-------
'11 . Zu
CHDALD	
	10 ¦ 66	lfl7Wi00
...... . i^gi9flR ni
	1323.62	
1 Qrt r\&. 
-------
rileNaat : C:\2700\GC3\HCF3023.raii	Data) 8/29/69 1:13 PH Paqe 1 of 1
Start Tiiwi 0.00 sin End Tiaa» 70.00 ain Lon Paint: 5148 uV High Paint: U4Z77 uV
Vertical Scale Factor: 0.00 Plat Offwt: 0 «V Plat Scale: 100 aV
ChroiatograB
¥
UMH
ttBH

« *8 3 sgssi	;nx»
k& xs ft a»»* mnucsss ssanxncdiia hi as
NiaitiaN • i
Trfit'rrj'i'i linn!
i Illllil s
.'I i i ¦ ¦ .^i ¦ i f. i i r. i ?¦ i .t. r. ¦ i iai
58,3
1LW	23.33	35.00
Til* (mis)
fleeted
C CC ' r *

-------
Nelson Analytical 2700 Chromatography System Report Header
is=sa3=a3=3aBa33=aaaaassa=3=B==sssssa3aa==3aass=aaassBaaaaaaassssaa=s
Sample Name : P803
Sample Number: 9S179
Operator	:
Time
Studv
8/29/89 2:25 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range s 1000
Data Acquisition Times 8/29/89 11:20 AM
Delay Time
Enc Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
In.i. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
m in.
min.
pts/sec
C:\2700\GC5\MCF5023. raw
C:\2700\GC5\MCF5023A. rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Re.iect	: 0.00
Area Threshold : 100
Multiplier	: 0.68
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
•3ol it Ratio
T smseraturs
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400 S
.25MM ID .23UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
15 PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 87
Ret Time
C m i n ]
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area Peak Ht Raw Amount
ug\L	CuV-secJ CuV3	ug'\L
11.63 B-BHG
¦4^ 4
;, nz
1523.33
90 .04

21.36 ALDI"
Ceo1''*

-------
¦10.35	DPP	9.Z7—11599. 50	iflqT.afl	17.73	f
4 4 >65	GNDOCULFATE	:	7-r-64	20552* 3-3	14604 55	11 j 19	
¦51.09 CNDKCTO	H-56	1912.40	125.01	1.05-.
61.43 DBC	319.12 353240.28 24493.72	469.30
Total Area = 980982.38
Total Concentration = 469.9491
Report by Doherty Bresnahan
eeettrSTw
CCO'^'

-------
FilaNaaa : C:\2700\GO\MCF3023.raM	Data* 8/29/89 2:2& PN Paga 1 oi 1
Start Tiaat 0.00 tin End Tia»« 70.00 ain Low Point) 5148 uV High Point: 114277 uV
Vortical Seals Factor: 0.00 Plot Offset: 0 oV Plot Scale' 100 aV
Chrcmatograi
1MH
ttja—

5 5»«H

; RS 3 5 W I?**	S«P*S*SW *3* 5?
-	! J SB XXK ass* «hk:9595 9;aft*H*R8S SSI II
.s»4 '
•'r hi ii i,i—iiiiii nirinirenn
[
sin
- u -
3 5 5-!
i	4JLJL1
I
. |
5 , r
a
1
~3U
1167	23.33	35.00	«.(7	S9.33
Tilt (ain)
000169- ¦90.
CCO I to

-------
80
PESTICIDE EVALUATION STANDARDS SUMMARY
tab Kane:	~/z	Contract:-.^'C 7 - Z299
Lab Coda:
Case No.:
~7
SAS No.
SDG No.:
Instrument ID: 'mJ&GG 'l*	GC Coluffl* 27^0/2V0/ Pirn
Dates o£ Analyses: *£/to ^7"?£
Evaluation Check for Linearity
PESTICIDE'
Aldrin_
Endrin"
4,4'-DDT
DBC
| CALIBRATION
| FACTOR
| EVAL MIX A
; | aanaasnan:
I///*? TCP -
7/9 7fg»g
 10.0% RSD, plot a standard curve and determine the ng
for each sample in that set from the curve.
Evaluation Check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)

INITIAL

oil
EVAL
MIX
B
02 |
EVAL
MIX
B
03 |
EVAL
MIX
B
04 1
EVAL
MIX
B
05 |
EVAL
MIX
B
06 |
EVAL
MIX
B
07 |
EVAL
MIX
B
08 |
EVAL
MIX
B
09 |
EVAL
MIX
B
101
EVAL
MIX
B
HI
EVAL
MIX
B
121
EVAL
MIX
B
13 |
EVAL
MIX
B
14 1
EVAL
MIX
B
DATE
ANALYZED

-------
3D
PESTICIDE EVALUATION STANDARDS SUMMARY
Lab Names LOCKHEED-ESC	Contracts 63-03-3249
Lab Code: Case No.:	SDG No.:
Instrument IDs VARIAN 3400 GC Column	IDs FSCCRTX5
Dates o-f Analyses 3—28-09 to 0-30-89
Evaluation Check •for Linearity
!	! CALIBRATION! CALIBRATION! CALIBRATION! */.RSD !
I PESTICIDE ! FACTOR	! FACTOR ! FACTOR	( I-f > 10.0'/. RSD? plot a standard curve and determine the ng
tor each sample in that set from the curve.
Evaluation Check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)
«
1
DATE
TIME
ENDRIN
4,4'-DDT
COMBINED
1
ANALYZED
ANALYZED


(2)
Jsaaassasasas
=sssas3ssss=
S = S33SSS33Sa
3SH33SS3SSS
========
=========
! INITIAL
3/28/89
0923
5.8
4.6

01! EVAL MIX B
8/29/89
0831
6.5
7 1
• »

02! EVAL MIX B
r*»— 1
8/30/89
0054
3. 1
4.7

1 i
04 !





05!





06 !





07!





OS!





09!





10!
¦




11 !





12!





13!





14!
1
l





(2) See Form instructions.
FORM VIII PEST-1
000182

-------
30
PESTICIDE EVALUATION STANDARDS SUMMARY
Lab Nana: Znc.£/\tr/ -/fZCL Contract
Lab Coda: 	
Case No.:
—7
SAS No.:
SDG No.:
Instrument ID: >//? 1 9nr, -dr
Dates of Analyses: *%/to
GC Column ID: 2^0/aVQ/jP^n
L/k?
Evaluation Check for Linearity
PESTICIDE
Aldrin	
Endrin	
4,4'-DDT
DBC	"
| CALIBRATION
| FACTOR
| EVAL MIX A
7 yy -rc-cc
7/9 -rccc
000

~>t £ COCO
Z A
4/C C/
/A~9
/ 7 10.0* RSD, plot a standard curve and determine the ng
for each sample in that set from the curve.
(1)
Evaluation check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)



tmm

INITIAL

Oil
EVAL
MIX
B
02 |
EVAL
MIX
B
03 |
EVAL
MIX
B
04 |
EVAL
MIX
B
05 |
EVAL
MIX
B
061
EVAL
MIX
B
07 |
EVAL
MIX
B
08 |
EVAL
MIX
B
09 |
EVAL
MIX
B
10 |
EVAL
MIX
B
HI
EVAL
MIX
B
12|
EVAL
MIX
B
13 |
EVAL
MIX
B
14 |
EVAL
MIX
B
DATE
ANALYZED
^M9A9
r/fc/^9
v
TIME
ANALYZED


ENDRIN
C
T~
Ll
(2) See Form instructions.
ooc \%
4,4'-DDT
J5LL
ZJL
~K7>6
COMBINED
(2)
FORM VIII PEST-1
8/87 Rev.

-------
3D
PESTICIDE EVALUATION STANDARDS SUMMARY
Lab Name! LOCKHEED-ESC	Contract! 68-03-3249
Lab Cade:	Case No.:	SDG No. :
Instrument ID: VARIAN 3400 GC Column IDs FSCCRTX5
- f
Dates of Analyse:8-28-89 to 8-30-89
Evaluation Check for Linearity

CALIBRATION!CALIBRAT ION!CALIBRAT ION
V.RSD
PESTICIDE
FACTOR
: FACTOR
FACTOR
< 10.OX RSO. plot a standard curve and determine ':r,a rvq
for eacn sample in that set from the curve.
Evaluation Check for 4,4'-DDT/Endrin Breakdown
(percent breakdown expressed as total degradation)


DATE
TIME
ENDRIN
4,4'-DDT
COMBINED


ANALYZED
ANALYZED


(2)

============
===========
=s==aas«saaa




INITIAL
8/23/89
0923
5.8
4. 6

01
EVAL MIX B
8/29/89
0851
6.5


02
EVAL MIX B
3/30/89
0054
S. 1
4. 7

. j
04






05






06






07






08






09


¦



10






11






12






13






14






(2) See Form instructions.
FORM VIII PEST-I
000182

-------
8E
PESTICIDE EVALUATION STANDARDS SUMMARY
Evaluation of Retention Time	Shift tor Dibutvlchlorendate
Lab Name: Lockheed-ESC	Contract: 68-03-3249
Lab Code: CASE *:	SDG No.:
Instrument IDs Varian 3400- '	GC Column ID: 2250/2401PK.D
Dates of Analyses: 3/29/89 TO 8/3|/89
: epa
: LAB SAMPLE
! DATE
1 TIME
i */.
i SAMPLE no.
! ID
! ANALYZED
1 ANALYZED
1 D
!============
j ============
| = = = 53 = = = ===
|===s=====a
1 =====
01:EVALA
!EVALA
18/29/89
1 1427
1 0.00
02:EVALB
:EVALB
18/29/89
1 1519
10.51
03!EVALC
:EVALC
13/29/89
1 1610
10. 12
04!INDA
i INDA
18/29/89
1 1702
1 0. 4o
05!INDB
i I NDB
!8/29/89
11754
10.31
06!TOXAPH
! TOX
18/29/89
1 1846
1 0.09
07!AR1660
!PCB1660
!3/29/89
1 1937
: o. 31
081AR1221
!PCB1221
!8/29/39
1 2029
10.31
0?!AR1232
!PCB1232
!3/29/89
1 2120
: o. 47
101AR1242
!PCB1242
13/29/89
1 ^ 4 ^
1 1 ~
1 0. 23
111AR1248
:PCB1248
!8/29/89
1 2303
10.53
12!AR1234
! PCB1254
:a/29/89
1 2356
1 0. 04
13!PBLK-1
!9S187RB
18/30/89
1 004y
10.35
14!PBLK-2
19S197RB
18/30/39
10139
10.27
15!0F01MS
!9S185MS
18/30/89
1 0230
1 0. 23
15 0F01DS
!9S186DS
18/30/89
1 0323
10.31
16!0F01
!9S177
18/30/89
1 0414
1 0. 23
17!EVALB
!EVALB
18/30/89
1 0506
10.39
13!0802
!9S178
18/30/89
1 0558
1 0. 12
I?!P303
!9S179
13/30/39
1 0650
1 0. 23
20!F1204
!?S180
13/30/39
1 0741
I O . 1 ^
21111205
!9S131
13/30/39
1 0833
l 0. 51
221M4A06
!9S132
13/30/89
1 0924
10,51
231INDA
i 100/'200A
18/30/89
1 1015
10.12
24!L4A07
!9S183
18/30/89
1 1212
10.16
25!M14A08
!9S184
18/30/39
1 1303
1 0. 19
26!H709
!9S188
13/30/89
1 1355
10
27!M510
!9S189
18/30/89
1 1446
1 0. 47
23!K411
i 9S190
18/30/89
1 1537
10. 19
29:EVALB
i EVALB
18/30/89
1 tltlS
1 f
301J212
19S191
18/30/89
1 1720
1 0.04
31:L513
19S192
18/30/89
1 1312
1 0. 08
32!D414
!9S193
18/30/89
1 1903
1 0. 04
33!P715
!9S194
18/30/89
1 1955
10.54
341 N116
!9S195
18/30/89
1 2046
! 0. 51
35!INDB
!100/200B
18/3(*/89
1 L-'l. | -5"
! o *
36!INDA
1100/200A
i
: oc
i o.crt
1
V / •
l
l
«
<
!
33:
1
1
l
1
t
i
* Values outsi
0.3% for cap
page 1 of 1
de of GC limits
illary columns)
FORM VIII PEST-2
(2.07. for packed columnsi
1/87 Rev
000183

-------
8E
PESTICIDE EVALUATION STANDARDS SUMMARY
Evaluation of Retention Time Shift -for Dibutvlchlorendate
Lab Names Lockheed-ESC	Contracts 68-03-3249
Lab Codes Case No.:	SDG No.s
Instrument IDs Varian 340&
34!0414
!9S193
13/30/89
0437
! 0.08
35!P715
I9S194
!3/30/89
0352
! 0. 11
36!N116
I9S195
!8/30/89
0706
10. 11
37!INDB
!100/200B
!8/30/89
.rQit
! 0. 24
38!INDA
!100/200A
18/31/89
0106
! 0.23
* Values outside of QC limits (2.0% -for packed columnsi
0.3"'. for capillary columns)
page 1 of 1	FORM VIII PESTq|jQ1Q4	1/87 Rev

-------
PESTICIDE/PCB STANDARDS SUMMARY
I
ab Name:,
Lab Code:
LOCKHEED-ESC
Case No.:
I
Contract:68-03-3249
SAS No.: 	
SDG No.:
nstrument ID; VARIAN 3400-t
GC Column ID:	/3 9ZV pfCQ

DATE(S) OF FROM:
ANALYSIS TO:
TIME(S) OF FROM: 1*Q 2.
ANALYSIS TO: 227b
DATE OF ANALYSIS
TIME OF ANALYSIS
EPA SAMPLE NO.
(STANDARD)
COMPOUND
RT
F
WIN
FROM
IT
rDow
TO
2.79
CALIBRATION
FACTOR
RT
CALIBRATION
FACTOR
QNT
Y/N
%D
alpha-BHC	
beta-BHC
2.76
2.73
14900000
4.07
4.03
4.11
4500645




delta-BHC
4.72
4.67
4.77
10600000




aamma-BHC
3.52
3 .48
3.56
11700000




Heptachlor	
Aldrin
4.33
4.29
4.37
10850000




5.21
5.16
5.26
12400000




Hept. epoxide
Endosulfan l—
Dieldrin
7.69
7.61
7.77
10150000




9.44
9.35
9.53
9600000




11.27
11.16
11.38
10800000




1 4.4'-DDE
10.85
10.74
10.96
9975000




1Endrin
13.22
13.09
13.35
6950000




Endosulfan II
4.4#-DDD
15.47
15.32
15.62
14025000




15.29
15.14
15.44
7725000




Endo. sufate
4.4'-DDT
21.40
21.19
21.61
4500000




17.67
17.49
17.85
4275000




Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane_
Toxaphene	
Aroclor-1016_
Aroclor-1221_
Aroclor-1232~
Aroclor-l242_
Aroclor-l248_
Aroclor-l254_
Aroclor-1260_
27.21
26.94
27.48
2635000




25.77
25.51
26.03
8025000




9.19
9.10
9.28
10500000




8.47
8.39
8.55
10350000




18.07
17.89
18.25
374762




4.3
4.26
4.34
322340




2.55
2.52
2.58
195860




4.3
4.26
4.34
153150




4.3
4.26
4.34
181334




5.44
5.39
5.49
299659




13.05
12 . 92
13.18
660939




21.08
20.87
21.29
716135







1



I
I
:.on was performed, N if not performed.
Under QNT Y/N: enter Y if quantitat
1;D must be less than or equal to 15.0% for quantitation, and less than
>r equal to 20.0% for confirmation.
fote: Determining that no compounds were found above the CRQL is a form of
[piant itation, and therefore at least one column must meet the 15.0% criteria.
For multicomponet analytes, the single largest peak that is characteristic
ff the componet should be used to establish retention time and %D.
dentification of such analytes is based primarily on pattern recognition.
page j__ of
FORM IX PEST	Q0018s	•/« Re

-------
9
PESTICIDE/PCB STANDARDS SUMMARY
Lab Name:	LOCKHEED-ESC	 Contract: 68-03-3249
Lab Code: 	 Case No.:	 SAS No.: 	 SDG No.:
Instrument ID: VARIAN 3400 - J	GC Column ID: 2250/2401PKD

DATE (S) OF FROM: 8/Q9 fA<*
ANALYSIS TO: R/J9/753
TIMEfS) OF FROM:
ANALYS IS TO: 23
DATE OF ANALYSIS 8/3 0/8y
TIME OF ANALYSIS 1015
EPA SAMPLE NO.
(STANDARD) INDA
COMPOUND
RT
2.76
F
WIfl
FROM
IT
mow
TO
2.79
CALIBRATION
FACTOR
RT
CALIBRATION
FACTOR
QNT
Y/N
aas
%D
saaas
alpha-BHC
beta-BHC
2.73
14900000
4.07
4 .03
4.11
4500645




delta-BHC
4.72
4.67
4.77
10600000




gamma-BHC	
Heptachlor	
Aldrin
3.52
3.48
3 .56
11700000
3.53
12500000
V
6.8
4.33
4.29
4.37
10850000
4.33
11800000
V
8 . 8
5.22
5.17
5.27
11550000
5.22
12250000
y
6 . 1
Hept. epoxide
Endosulfan I_
Dieldrin
7.69
7.61
7 .77
10150000
7 .68
10800000
V
6 . 4
9.44
9.35
9.53
9600000
9.43
10200000
y
6. 2
11.27
11.16
11.38
10800000
11.is
11500000
y
6. D
4.4'-DDE
10.85
10.74
10.96
9975000


/
i

Endrin
13.22
13.09
13.35
6950000



Endosulfan II
4.4'-ODD
15.47
15.32
15.62
14025000
15.42
15050000
7 . 3
15.29
15.14
15.44
7725000



Endo. sufate
4.4'-DDT
21.40
21.19
21.61
4500000



17.67
17.49
17.85
4275000
17.61
4525000
5. 8
Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane_
Toxaphene	
Aroclor-10l6_
Aroclor-l221~
Aroclor-l232_
Aroclor-1242~
Aroclor-1248~
Aroclor-1254_
Aroclor-1260~
27.21
26.94
27.48
2635000
27.05
2700000
2.5
25.77
25.51
26.03
8025000



9.19
9.10
9 .28
10500000



8.47
8.39
8.55
10350000




18.07
17.89
18.25
374762




4.3
4 .26
4.34
322340




2.55
2.52
2.58
195860




4.3
4.26
4.34
153150




4.3
4.26
4.34
181334




5.44
5.39
5.49
299659




13.05
12.92
13.18
660939




21.08
20.87
21.29
716135












Under QNT Y/N: enter Y if quantitation was performed, N if not performed.
%D must be less than or equal to 15.0% for quantitation, and less than
or equal to 20.0% for confirmation.
Note: Determining that no compounds were found above the CRQL is a form of
quantitation, and therefore at least one column must meet the 15.0% criteria.
For multicomponet analytes, the single largest peak that is characteristic
of the componet should be used to establish retention time and %D.
Identification of such analytes is based primarily on pattern recognition.
page <2. of
FORM IX PEST 000186	a/87 Re

-------
PESTICIDE/PCB STANDARDS SUMMARY
Lab Name:,
Lab Code:
LOCKHEED-ESC
Contract:68-03-3249
Case No.:
SAS No.:
SDG No.:
Instrument IP; VARIAN 3400-1
GC Column ID: 2250/24Q1FKD
COMPOUND
alpha-BHC_
beta-BHC
delta-BHC	
gamma-BHC	
Heptachlor	
Aldrin	
Hept. epoxide
Endosulfan I_
Dieldrin	~
4,4'-DDI	
Endrin	
Endosulfan II
4,4'-DDD	
Endo. sufate
4,4' -DDT		
Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane__
Tox'aphene	~
Aroclor-1016_
Aroclor-1221_
Aroclor-1232_
Aroclor-1242~
Aroclor-1248_
Aroclor-1254~*
Aroclor-l260~
DATE(S) OF	FROM
ANALYSIS	TO
TIME(S) OF	FROM:
ANALYSIS	TO:
« /la)9 (£9
	
	ZHStp
RT
2.76
4.07
4.72
3.52
4.33
5.21
7.69
9.44
11.27
10.85
13.22
15.47
15.29
21.40
17.67
27.21
25.77
9.19
8.47
18.07
4.3
2.55
4.3
4.3
5.44
13.05
21.08
RT
WINDOW
FROM TO
2.73
4.03
4.67
3.48
4.29
5.16
7.61
9.35
11.16
10.74
13.09
15. 32
15.14
21.19
17.49
26.94
25.51
9.10
8.39
17.89
4.26
2.52
4.26
4.26
5.39
12.92
20.87
2.79
4.11
4.77
3.56
4,37
5.26
7.77
9.53
11.38
10.96
13.35
15.62
15.44
21.61
17.85
27.48
26.03
9.28
8.55
18.25
4.34
2 * 58
4.34
4.34
5.49
13.13
21«29
Under QNT Y/N: enter Y if quantitat
CALIBRATION
FACTOR
14900000
4500645
10600000
11700000
DATE OF ANALYSIS 8/31/89
TIME OF ANALYSIS 00T5
EPA SAMPLE NO.
{STANDARD)	IND8
RT
2.77
4.08
4.74
10850000
12400000
10150000
9600000
10800000
9975000
6950000
14025000
7725000
4500000
4275000
2635000
8025000
10500000
10350000
374762
322340
195860
153150
181334
299659
660939
716135
5.23
10.87
13.23
15.33
21.43
25.76
9.21
8.49
CALIBRATION
FACTOR
17300000
5100000
12400000
13700000
11000000
7050000
8900000
4975000
7350000
11400000
11450000
QNT
Y/N
sssa
JL
T^—'
V
31
%D
16.1
13.3
trra

IZI
£
z
z
;.on was performed, N if not per
10.5
10.3
T7

1076
8.4
8.6
10.6
ormed.
%D must be less than or equal to 15.0% for quantitation, and less than
or equal to 20.0* for confirmation.
Note: Determining that no compounds were found above the CRQL is a form of
quantitation, and therefore at least one column must meet the 15.0% criteria.
For multicomponet analytes, the single largest peak that is characteristic
of the componet should be used to establish retention time and %D.
Identification of such analytes is based primarily on pattern recognition.
page 3 of	nflfVfOT	„ „
FORM IX PEST	UUUlO#	8/87 Re

-------
9
PESTICIDE/PCB STANDARDS SUMMARY
Lab Name:
Lab Code:
T .QCKHEED—ESC
Case Ho.:
Contract:68-03-3249
SAS No.: 	 SDG No.:
Instrument ID: v&rtrn 34.00-i
GC Column ID: 2250/2401PKD
DATE(S) OF
ANALYSIS
TIME(S) OF
ANALYSIS
FROM:	a/ooTwr
TO:	& /<0.0/&Q
FROM:	/4-OZ
TO:
COMPOUND
RT
F
win
FROM
2.73
IT
(DOW
TO
2.79
CALIBRATION
FACTOR
14900000
RT
CALIBRATION
FACTOR
QNT
Y/N
%D
alpha-BHC
beta-BHC
2.76
4 .07
4.03
4.67
4.77
4500645


~
- V
V
~-Z
¦

delta-BHC
4.72
10600000



gamma-BHC	
Heptachlor	
Aldrin
3 . <52
3 .48
3.56
11700000
3.54
13100000
12 . 0
4.33
5.22
4.29
4.37
10850000
4.34
12450000
14.7
5.17
5.27
11550000
5.22
12250000
6.1
Hept. epoxide
Endosulfan l_
Dieldrin
7.69
7.61
7.77
10150000
7.69
10700000
5.4
9.44
9.35
9.53
9600000
9.43
10050000
4.7
11 .27
11.16
11 ¦ 38
10.96
10800000
11.29
11225000
3.9
4.4'-DDE
10.85
10.74
13.09
9975000


Endrin
13.22
13.35
6950000


£
5

Endosulfan II
4.4'-DDD
15.47
15.32
15.14
15.62
14025000
15.42
14175000
1.1
15.29
15.44
7725000



Endo. sufate
4.4'-DDT
21 .40
21 .19
21.61
4500000



17. 67
17.49
17.85
4275000
17.62
5875000
37 . 4
Methoxychlor-
Endrin ketone
a. Chlordane_
g. Chlordane~
Toxaohene
27.21
26.94
27.48
2635000
27.10
3125000
18. 6
25.77
9.19
25.51
9.10
26.03
8025000



9.28
10500000



8-47
8.39
8.55
10350000




7 ft. 07
17.89
18.25
374762




Aroclor-1016_
Aroclor-1221_
Aroclor-1232_
Aroclor-1242_
Aroclor-1248~
Aroclor-1254_
Aroclor-1260_
4 . 3
4.26
4 . 34
322340




2 . 55
2 . 52
2.58
195860




4 . 3
4 . 26
4.34
153150




4 . 3
4 . 26
4.34
181334




5.44
5.39
5.49
299659




1 3 . 05
12 . 
-------
9
PESTICIDE/PCS STANDARDS SUMMARY
Lab Name:
i nn-'HFPn-pqr.


Con t r ac t: 60-03-3"?
49
Lab Code:
Case No.
•
¦

SAS No.!

SDS No.:
Instrument ID'_
Kjap t AN
ZMLQ-*"


GC Column
IDs _£
SrCRTX*

DATE(S) OF
FROM!
a-
-9B-Q9
DATE OF ANALYSIS !

ANALYSIS
TO*.
R-
-3A-M
TIME OF ANALYSIS s

TIME(S) OF
FROM 8
0809
EPA SAMPLE NO. !

ANALYSIS
TO!
iiia?
(STANDARD) !







»
i
i

RT




i I
i I
! COMPOUND
RT
WINDOW
CALIBRATION
RT
CALIBRATION
ONT: %D !
t
1

FROM
TO

FACTOR

FACTOR
Y/N! ;
! aleha-BHC
lO.'t
1 0. '20
10.34

231 4*9=1


i •
i >
! beta-BHC
It.**






• i
i t
!delta-BHC
14. 15
14. 13


1736730


t i
t
1aamma-BHC
12. 33
12.33

201=980


i i
i I
!Heptachlor
18. 12
18. 07
18. 17
968875


i *
4 4
1 A1dr i n

21.48
21.54

2023540


1 t
1 t
!Hept. epoxide
26. OS
26.00
26. 10

140460S


1 <
1 1
!Endosulfan I
30. 37
30.35
30.39

1 *f 1 QB'IA


1
1 1
!Dieldr in


33.83

711188


1 1
t i
'.4,4*-DDE
34.54
34.52
34.56
1484860


1 1
» »
!Endr in
36. 68

36 .as
4374SO


i *
1 1
1 Endosulfan II
38. 11
30.08
39. 14
1144315


1 1
I 1
! 4. 4-' -DDD
40.47
40. 45
40.49
529625


i i
t 4
!Endo. sufate
44.59
44.57
44.61
Q09498


1 4
1 *
;4.4'-DDT
45 _ 3?
45. 92
46.02
"T C ^ O "7 CT
/ W 'mi / W


1 1
t i
\ i1etho;;vch lor-
55.94
55.39
55. 99
9230lO



!Endrin ketone
51.22
51. 19
-"¦ner
51 •
516505



: a. Chiordan©
30.95
30.93
30.97
1697540


1
1
! q. Chlordane_
28.99
28.97
29.01
1685680


t
1
1 To;;aphene
50. 64
50.53
50.75
70977


)
1
1Aroclor-1016
19.91
19. 88
19.94
254733


t
1
!Aroclcr-1221
10.31
10.26
10.36
85181


I
I
i Aroclor-1232

13. 12
13.30
118604


1
! Aroc lot—1242
17.74
17.64
17.84
200099


f
1
1Aroclor-1248
^>"7 T/L

27.49
249761


I
1
!Aroclor-12S4_
35.3
35. 18
35.42
273546


<
1
1Aroclor-1260
57. 14
57.02
57.26
422693


1
1
i
i






*
1
Under QNT Y/Ns enter Y if quantitation was performed* N if not per formed.
%D must be less than or equal to 15.OX for quantitation, and less than
or equal to 20.0"/. for confirmation.
Notes Determining that no compounds were found above the CRQL is a form of
quantitation, and therefore at least one column must meet the 15.0" criteria.
For ntul t icomponet analytes. the single largest peak that is char actor i st ic
of the componet should be used to establish retention time and %D.
Identification of such analytes is based primarily on pattern recognition.
, 4	0(30189
page J_ of T_
FORM IX F'€ST	a .'37 *e>

-------
9
PESTICIDE/PCS STANDARDS SUMMARY
Lab Names	< nrmccn-ger	 Contract;Aa-AT-2?ag
Lab Codes 	 Cass No. s	 SAS No. i _______ SDG No. s
Instrument IDs	-rami -g"	SC Column IDs Fgrri?TY^

DATE(S) OF FROMJ
ANALYSIS TO: o-M.ao
TIME 	"TJ.
CALIBRATION
FACTOR
RT
CALIBRATION
FACTOR
QNT
Y/N
7.D
beta—BHC
^ 1 3S
1 i eq! 1 •-> 1
79 "JO-TO:



¦del ta-BHC

1-1 t I \ J. T7
»?T.A7-rn



aamma-BHC
, _.a
1 "> " '• 1 ^ J."
->A 1 AQSA
1 2 ... 27
1 7 7 A37.5
/£	
/-•
/
! 1 . •?
Hep tachlor	
A1dri n
i a 1 2
,rs cit! is.17
a^ap.7=:
1 9. 1 S
1 AS44SC")
"M si
¦71 AR > SA
^A775AA



Hgpt. sPOKide
Endosulfan I_
D i e1dr i n
">a , as

14A4AA5
7A._ OS
1 -^srs

7111SB
72. B7
90OA1S

4. 4'-DDE

74 52 I 74 . SA
1aSdBAft


Endr in


4374SA !


Endosulfan II
4,4'-DDD
T.B. 1 1
7R.AR! 7R.14
114431 5
3fl. 12
957570

. 16*5
40. 47
40_ 45 i AC,. 49
529A25


Endo. sufate
44 . S9
44 . "57 ! 44. A 1
0AO40S


. Z
—. «b *
;4*-0DT
<15. <97
a«,.o-?! 4A.D2
?ceo
45.°-S-
—S. 92
	S41745
!MgthCKVChlor —
SS. "54
55.39! W.oo
°--3aio
;Endrin ketone
5 a. Chlordane_
:-a. Chi or dan e_
! To:2! 57. 2A
422A9S



I I
1 1




Under QNT Y/Ns enter Y if quantitation was performed. N if not performed.
7.D must be less than or equal to 13.07. for quantitation, and less than
or eaual to 20.07. for confirmation.
Note! Determining that no compounds were found above the CRQL is a form of
Quantitation* and therefore at least one column must meet the 15.07. criteria.
For multicomponet analytes. the single largest peak that is characteristic
jf the componet should be used to establish retention time and "D.
Identification of such analvtes is based	Patterri r®co<3nltion-
age J? of Lj^_
FORM IX PEST	3/87 Re

-------
9
PESTICIDE/PCB STANDARDS SUMMARY
_ab Name»
Lab Code:
nn-uFcn-cgp
Case No.:
Instrument IDs
Contract;
SAS No. s 	 SDG No.:
GC Column IDs garpBTyw
COMPOUND
alPha-BHC
beta-BHCJ
delta-BHC.
qamma-BHC
Heptachlor	
Aldr in	
Hept. epoxide
Endosulfan I_
Dieldr in
4,4'-DDE	
En dr i n	
Endosulfan II
4,4'-ODD	
Endo. sufats
4, 4'-ODT_	
r-iethoxychlor-
Endrin ketone
a. Chlordane_
q. Chlordane_
Taxaphene
Aroclor-10l&_
Aroclor-l221_
Aroclor-1232_
Aroc loi—1242_
Aroclor-1248_
Aroclor-1254_
Aroclor-l260_
DATE(S) OF	FROM:
ANALYSIS	TO:
TIME(S) OF	FROM!
ANALYSIS	TO:
fl.-2aTB9.
-SaS%sSSL
t'iart9	
i-i 1 a jT	
RT
10.31
i;. 93
:a
is. i:
M A7
24-OS
•n ~7

mm2JXrnmhJBL
~R. 11
4Q. 47
44-
Afi.<97
¦^.U ¦ 95
IS. 99

I?i 91
10.51
13 "M
iliiZit? 4
27.56
35.:
57,14
RT
WINDOW
FROM ! TO
10» 54'
11. 9.5

tg.c»7
71 A?
:h. nn
10-

L6l—6B
"R.OS
40. 4S
44.57
45.
30.9:
£8.. 77
su - —
li 9 ¦
A£LJZt

12
17.64
,,,<¦/ » AW
-.•5 .IS
57.02
-04-
14.	17
-t:
IB, 17
X.

n 39
.83
-A.fla
iR >14
4Q. 49
44. At
02
,.JW.
22
LU25
70. ?7
29.01
.aa
22
	17.94
10. -7 a
1 »-5C
17.94
17,**
.-5.4^
37.1b
¦iflUbwpvMUP
CALIBRATION
FACTOR
	3114695
-zss:
-L
2C) 14380
-S4ae2S-
'141'
1 404605
131R^7n
7111 SB
lAflARAO
*374*«->
1 14**1'
•?9A7'
QH949P
lazzn
"mo
iiASQ;
1£97540
1685680
u.
Q977
S477!
85131
11 SAO4
£0009*1
249761
.¦7>*,w^6
422695
DATE OF ANALYSISfl-7i-i-aq
TIME OF ANALYSIS?^?
EPA SAMPLE NO.
(STANDARD)	t imps
RT
lii.
II.90.
14. 04.
v4.,7R
40. 29
4^.41
il.V4
28.35
CALIBRATION:0NT
FACTOR IY/N
¦ SS33S33
;a9&oo
HZiO-
-LZSlMAO-
i4inr
.709515-
1619895
7.D
.¦ la
Under QNT Y/N: enter Y if quantitation was performed, N if not performed.
%D must be less than or equal to 13.07. for quantitation, and less than
or equal to 20.07. for confirmation.
Note: Determining that no compounds were found above the CRQL is a form of
uantitation. and therefore at least one column must meet the 15.0% criteria.
3r multicomponet analytes, the single largest peak that is characteristic
¦ the componet should be used to establish retention time and *'.D.
lentification of such analytes is based priQOttlSI pattern recognition.
iae
y>
Qi
1
FORM IX PEST
}/S7 Re

-------
9
PESTICIDE/FCB STANDARDS SUMMARY
Lab Name»_
Lab Codes
Instrument
' nr^uccn-ccr
Case No.:
Con tract:
SAS No. s 	 SDG No. :
GC Column IDs cirrgrve:
! DATE 
OF
FROM: q-?o-flo
: DATE OF ANALYSISn-^i!-R9
1 ANALYSIS

TO: -hq
! TIME OF ANALYSIS^ 1,-,^
! TIME(S)
OF
FROM:
! EPA SAMPLE NO.
! ANALYSIS

TO: nOC	
! (STANDARD) Tuna
<
l
COMPOUND
a 1pha-BHC.
aeta-BHC
de I ca-BHC
!	RT
RT ! WINDOW
! FROM ! TO
CALIBRATION
FACTOR

; i. X\

14. i;
M-
aamma-BHC
17
33 :
1 *¦» T"^ !
1 ~,
• ^ '
Heptach lor		
—1-3-f

i3.i:>7;.
13,
-IZ:
A1dr i n
71
51 !
19!
'"I
^4 1
Hept. epoxide

;!
7 a i*i i-i!
76
1 •
Endosulfan I
'1*1
T7 ¦
TA T®! !

-9 i
D i e 1dr i n

fl? 1
79i
"T T
ss!
4.4'-DDE
TA-
«14!
T4 . !
14.
=:a :
Endr in
TA.
Afl >
ta.ab!
16.
ftfli
Endosulfan II

1 i ! t:r . on!
za.
.14:
4,4'-DDD
40.
47 '•
40.45:
4<">
49:
Endo. sufate
44.

44.^7:
44.
61 :
4.4' -DDT
4«3.
07 !
as.9?!

('(7 !
;ietho::vch lor-
ss.
94 i
¦=•>5.99!
"ifi
99:
Zndrin ketone

.22:
=11.19!
=\\
23!
a. Chlordane


y.a.9y.\

97 !
a. Chlordane

99!
?s.97:
¦-•9
01 !
Toxaphene
!W
Ml
«=:<•). Fi!\:
TiO
.73!
Aroclor-1016_
19.911
17.88!
i?
¦ 74!
Aroclor-1221
10.
~1 !
1CJ.7A!
1 <">
.36!
Aroclor-1232

71 *
1^.1?:
1*
10!
Aroclor-1242
17
74!
17.A4:
17
R4!
Aroclor-124B
17


77
49!
Aroclor-1254
?.X. 3!
is. m!
ifi
. 4?:
Aroclor-1260
S7
14:
^7.09!
f!7
.?5C>??5
1 IZ*-£JSl
ONT
v/n
/>
*/.D
JJ
— 1. 5
0.7
",8. (V
9. 9
^L.,.4
Y i f
Under ONT Y/N: enter
*/.D must be leas than or equal to 15
or equal to 20.0'/. for confirmation.
quantitation was
0'/. tor
performed. N
quant i tat ion 1
if not per
and less
forme
than
d.
Note! Determining that no compounds were + ound above the CROL is a torm of
quant i tat ion» and therefore at least one column must meet the 15.07. criteria.
For mult icomponet analytesi the single largest peak, that is character ist ic
the componet should be used to establish retention time and /CD.
o+
Identification of such analytes is based pr^
page of ^
Jn pattern recognition.
FORM IX PEST
3-^1=7 Re

-------
10
FESTICZDE/PCB IDENTIFICATION
EPA SAMPLE MO.
r
Lab Nana: 1	. Contract: (c%. 'C3	^	|
Lab Cod#:
Caaa No.
SAS No.:
SDG No.:
GC Column ID (1):	R£-0	qc Coluan ID (2): F^ZCCTCifT
Inatruaant ID (1):	^ I	Inatrumant ID (2):	3>KX)*b^'
Lab Saapla ZD:
Lab Fila ID: __________	(on*Y	confirnad by GC/MS)
PESTICIDE/PCB
RETENTION TIME
01	^ ^ ' - CdO^- Coluan 1 1 c-^
02	Coluan 2 3<4. ^
RT WINDOW
OF STANDARD
From to
IC.1+ /c/i L*
3
-------
-pO-4U iC&O
&COIert'*-

-------

L<-

f
U| + h(jL~^k
QOC(c^"

-------
l^-f" blt^Jc.
u£oiciL

-------
		r f	,
' ^^0	lC^O	if
C'CCKi^

-------

OOCI^S"

-------
a?*0 ;^+,r^
lvl+ !sLa~JC.
OCO Ic'c'

-------

ooo^°

-------

QCO i 0 *

-------
pivc/)	(_ LV^X) <	I I CW4
•j?ccac 5.

-------

<0 CO -i. C ~L

-------
bLz	k.
Occ'^c^

-------
—rW> .pi4U. lO&g *
b-if bLc^J<.
£C O ic ^

-------
C^X<0	i	i	C*v\ct-^X^
4
CGPCu

-------
"TWp^u. LO*«
Ooc^t^-

-------

OCCl°^

-------

cc-ojia

-------
Sample Name : EVALA
Sample Number:
Operator : tar
Nelson Analytical 2700 Chromatography System Report Header
7:38 AM
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
2:27 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount
e:\pkd\MCFR0 0 6.raw
e:\pkd\MCFR006.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL"
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
R«c Tlaa
Caiymm
Adjusted Amount
Rav Amount
P«ak Art*
Peak flt
MULTIPLIER
[mini

UG/L
UG/L
[uV-sac)
[uV]
Adi/Raw
3.2*
AL0RIH
0.00
0.00
232993.00
16963.2

13.2*
ENDftXH
0.00
0.00
148940.00
3147.2

13.3*
000
0.00
0.00
12290.00
367.9

17. «*
00T
0.00
0.00
73940.00
2119.3

23.69
08C
o.oo
0.00
113443.00
2696.1

Total Aria • 381610.00
Total Caoeaatratloa - 1.0000
Report by Tim Rand, Lockheed-ESC
000210

-------
FileNane : e:\pkd\HCFR006.rau	Date: 8/30/89 7:38 AH Page 1 of 1
Start Tine: 0.00 ain End Tiae: 47.00 Bin Low Point: 9190 uV High Point: 327490 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 OV Plot Scale: 2S0 mV
d_»
cr>
c/i
<3->
250.000-
208.333-
166.667-
125.000-
83.333-
o
o
o
ft *1.667-
-0.000-

A

"3
vn
Ol
(D
mS
CN
¦fV rr^T

I I
te! H S
Pi i Ht
&
I I I I I l"l I I | I I IT I l*T I i
7.83	15.67
I I I
T
23 . 50
Time (min)
I I I I I | l I I l I l
31. 33
I | I I I r
39.17
I I I

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : EVALB
Sample Number:
Operator : tar
Time
Study
8/31/89 2:05 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time	:	0.00 min.
End Time	:	47.00 min.
Sampling Rate :	1.0 pts/sec
3:18 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR007.raw
e:\pkd\MCFR007.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*EXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Sac Tlaa Co^onaat Adjusted Aoount Raw Amount	Paak Araa	Peak He	MULTIPLIER
[min) Naaa	UG/L	UG/L	(uV-»ac|	[uV]	Adj/Raw
3.22 AURIM	0.00	0.00	1.22*6	S8332.ll		
13.26 EHDRIB	0.00	0.00	696223.44	24604.63		
15.36 DSD	O.OO	0.00	72283.00	2133.88		
17.69 DOT	0.00	0.00	297440.00	S668.89		
23.82 0BC	0.00	0.00	641260.00	14232.10		
Total Araa - 2928104.30
Total Concentration • 1.0000
Report by Tim Rand, Lockheed-ESC
000212

-------
Chromatoaram
FlIeNane : «:\f*d\MCF*007.r»w	Date: 8/30/89 7:44 AM Page 1 of 1
Start Tlaa: 0.00 aln End Tfne: 47.00 -In Low Point: 5710 uv High Point: 223570 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 MV Plot Scale: 250 mV

250.000-
c-w to
CN to
kT> ¦£>
CO tO CTI
c^( ir» to
•—» v> r-»"
Ch
*n,
\3
Of
&
o
CO
CL>
CxL
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000
JH
Sr
t	r
A
rA
C3
e»
i	ii	it



I I I I I I I I I I I I I I I
7 .83
fi i^iFi i Fil
&
15. 67
i i i i i i i i i n i i i i i i j i i i i i i i i i | i i i i i i i i i
23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : IVALC
Sample Number:
Operator : tar
Time
Study
8/29/89 5:35 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/235
10000
Data Acquisition Time: 8/29/89
Delay Time : o.oo min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
4:10 PM
Raw Data File	:
Result File	:
instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR008.raw
e:\pkd\MCFR008.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.sap
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Rej ect
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Hat Tim	Consonant	Adju.e.d Anoint lUw Amount Paak Ar.» Faak Ht KULTIFtlER
'slal	Haaa	UO/L	UG/L Jutf-«ael CuV] AdJ/ttaw
5.21 ALDSSIH
0.00
0.00
2.*3«6
181626.89

10.93 ODE
0.00
0.00
20130.00
629.33 -

11.22 EOT«H
0.00
3.30
1.41.6
*90*0.98

13.3* ODD
0.00
o.oo
318933.33
3090,07 -

17.SI DDT
0.00
o.oo
•2003*.S3
21126.99

2t.io amia
0.00
0.00
197893.86
*167.81

11.66 0BC
0.00
0.00
1.33.6
29229.83 -

fetal Araa m 6380*90.00
Total Caneaatratlea " 1.0000
Report by Tim Rand, Lockheed-ESC
000214

-------
FileMaoe : e:\pkd\MCFB008.raM
Start Tlae: 0.00 ain End Tlae: 47.00 ain
Vertical Scale Factor: 0.00 Plot Offset:
Date: 8/29/89 5:35 PH Page 1 of
Low Point: 5550 uV High Point: 265620 uV
0 bV Plot Scale: 250 mV
Chromatogram
a>
cr>
CO
a*
O
O
o
n
C/l
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
irt
5
ts
id
ro cs 75:
3 £} 3


-^n^r
^ H s
i i.i . f~j>
i i i r3? i i | i i i? i iT i i H i i i i i
to
T Is? I
7.83
V
15.67
23 . 50
Time (min)

T-r
i 'p-1! I I I I I I i i | i I i i I i i i
31.33
39.17

-------

/
5
m
a
i
r?0
C£"" {,¦
<- f C C„

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : INDA
Sample Number: 100/200A
Operator : tar
Time
Study
8/30/89 7:12 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
5:02 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR009.raw
e:\pkd\MCFR009.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
0.00
*EXTERNAL STANDARD REPORT'
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
(mini
Cacponant
Adjuatad Amount Raw Amount Paak Araa Paak He
UC/L	VG/L . [uV-i«e) (uV)
MULTIPLIER
AdJ/Raw
3.32 C-BHC
100.00
100.00
2.34*6
262247
88
1.00
4.33 HPTCHLR
100.00
100.00
2.17.4
194337
48
1.00
3.22 ALOUD
100.00
100.00
2.31a6
172399
19
1.00
7.69 HEPEPOX
100.00
100.00
2.03*6
108289
73
1.00
9.44 ENDOl
100.00
100.00
1.92*6
83268
70
1.00
11.27 DIELDRIH
200.00
200.00
4.32*6
168198
41
1.00
15.47 ENDOl
200.00
200.00
3.61*6
166490
39
1.00
17.67 DOT
200.00
200.00
1.71*6
49103
94
1.00
1S.SS EHDAL8
200.00
200.00
2.62*6
33870
09
1.00
23.80 DBC
200.00
200.00
2.66*6
37072
61
1.00
27.21 MEIH0XT
1000.00
1000.00
3.27*6
120386
83
1.00
Total Araa - 3300)344.00
Total Concentration - 2500.0000
Report by Tim Rand, Lockheed-ESC
000216

-------
Chromatoqram
FileNaae : e:\pkd\MCFB009.ray	Date: 8/30/89 7:13 AN Page 1 of 1
Start Km: 0.00 ain End Km: 47.00 ain Lou Point: 5310 uV High Point: 265190 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 «V Plot Scale: 250 aN
r— po	o	o	o *—
u> Dq	(«->	r><	oo
l-s cd	-—	V	yS
«— -—	cn	og «r-«
250.000
208.333
166.667
125.000
-0.000
7.83	15.67	23.50	31.33	39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface #
AutoSampler
Rack/Vial
INDB
100/200B
tar
Time
Study
8/30/89 7:15 AM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
5:54 PM
Raw Data File
Result File :
Instrument File:
Process File
Sample File
Sequence File
Inj. Volume :
Sample Amount
e:\pkd\MCFR010.raw
e:\pkd\MCFR010.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
0.00
kEXTERNAL STANDARD REPORT"
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Rot Tlao
Caoponant
Adjuatad Amount
Raw Amount
P*ak Ar*a
Peak Ht
MULTIPLIER
(in In)
Nana
UG11
UG 11
[uV-iacj
[uV|
Ad)/Raw
2.76
A-BBC
100.00
100.00
2.98*6
429283.2
1.00
4.07
B-BHC
100.00
100.00
900129.13
80946.6
1.00
4.72
D-BBC
100.00
100.00
2.12*6
178263.>
1.00
3.21
ALDRIN
100.00
100.00
2.48a6
181232.8
1.00
8.47
G-CHLDANI
100.00
100.00
2.07*6
101306.9
1.00
9.19
A-CSLDANX
100.00
100.00
2.10*6
92830.6
1.00
10.81
DDE
200.00
200.00
3.99*6
161777.8
1.00
11.12
esduh
200.00
200.00
2.78*6
96660.3
1.00
13.29
000
200.00
200.00
3.09*6
94)38.4
1.00
21.40
EHSOSULTAIX
200.00
200.00
1.80*6
42083.1
1.00
23.77
0BC
200.00
200.00
2.23*6
64019.4
1.00
26.22
mumu
200.00
200.00
3.21*6
70342.6
1.00
local Ar*a - 297908*2.00
Total Concentration «¦ 1800.0000
Report by Tim Randf Lockheed-ESC
000218

-------
Chromatogram
FIleNane : e:\pfcd\HCFRO10.raw	Oate: 6/30/89 7:15 AM Page 1 of 1
Start Tine: 0.00 ain End Tlae: 47.00 ain Low Point: 6130 uV High Point: 434150 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 M Plot Scale: 250 mV
Qj
CTt
CO

V iTl
CNI CN

i i*i fi i i i |'"f i 1*1* i iti r~j i
7.83	15.67
I I I I Vdl I J I I'T* I I I I l l | I I I I I I
23.50	31.33
I I | I I I I
39.17
TT

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : TOXAPH
Sample Number: TOXAPHENE
Operator : tar
Time
Study
8/30/89 12:14 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
6:46 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File
Sequence File	:
Inj. Volume	:
Sample Amount
e:\pkd\MCFR011.raw
e:\pkd\MCFR011.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 100.00
********** PCB/TOXAPHENE STANDARDS REPORT *****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Peak Ret Time	Component	Peak Area Peak Ht BL

[min] Name
[uV-sec]
[UV]
Type
1
1.53
12785.00
1.00
BB
2
2.74
4940.00
554.03
BB
3
5.68
15669.72
714.39
BV
4
6.67
25647.33
1328.33
W
5
7.77
37350.88
1293.16
VB
6
9.11
54650.00
1604.76
BB
7
11.22
151458.13
4507.26
BV
.8
12.33
125657.13
2690.70
W
9
13.04
98261.99
2786.75
W
10
13.96
32484.75
1004.78
VB
11
14.83
49962.95 •
1960.55
BV
12
15.63
225553.19
5954.49
VB
13
16.83
43039.86
1480.79
BV
14
18.07TTX
374762.56
6546.22
W
15
19.28
130638.75
2475.72
VB
16
21.19
266583.91
5837.48
BV
17
22.51
227388.50
3494.33
W
18
24.10
150732.31
3613.98
VB
19
25.71 V-C
1.21e6
26556.20
BB
Total Area = 3245562.00
=™™=«=============	==e===M====_===		QQQ22Q

-------
REPORT BY TIM RAND, LOCKHEED-ESC
000221

-------
cnromauouram
fiIcMaoe : e:\pkd\HCfR011.raw	Date; 6/30/69 12:14 PH Page 1 of 1	^
Start Tine: 0.00 ain End lias: 47.00 ain Lom Point: 4160 uV High Point: 91770 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 60 mV
*¦n
oa r— -m— cm —h->	ki oa	en t—	¦—-	i—
<3 r^. t- cw o	do	era qcs	r- m	r-
krt r—en —	id 3 erf	- pJ	-*=r	uS
—	-—	-—	-— •— «—	TN CM	CN	CM
60.000-
Oj
cr>
cry

CXl
50.000-
40.000-
30.000-
20.000-
10.000-
0.000-
H
Trf
O
o
o
ro
M
ro

i | i I I i I I I i i [ i I I i i i i i T j i i i i i i i i i j i i i i I i i i i
15.67	23.50	31.33	39.17
Time (min)
I l l I I
l | l I I I I I i I
7.83

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1660
Sample Number: PCB1660
operator : tar
Time
Study
8/30/89 12:16 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
7:37 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	;
Sequence File	:
inj. Volume	:
Sample Amount	;
e:\pkd\MCFR012.raw
e:\pkd\MCFR012.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.sop
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
100.00
********** PCB/TOXAPHENE STANDARDS REPORT *********
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401

Peak
Ret Time
Component
Peak Area
Peak Ht
BL
#
[min]
Name
[uV-sec]
[UV]
Type
1
1.55

15640.00
1.00
BB
2
2.24

27106.38
2945.03
BV
3
2.55

123957.23
15076.48
VB
4
3.31

162595.00
17565.45
BB
5
3.85

69210.00
5408.54
BB
€
4. 20/*'6

322340.06
31442.95
BB
7
5.42

229050.00
8750.07
BB
8
6.37

17309S.45
9958.94
BV
9
6.78

162095.36
8388.17
VB
10
7.47

47090.44
2857.22
BV
11
8.13

145346.31
4522.32
W
12
8.94 >

115794.63
4892.16
VB
13
10.97

33959.34
1250.66
BV
14
11,92

330726.88
6878.43
W
15
13.01

305892.28
10403.82
W
16
14.36

657188.25
18789.72
VB
17
15.77

374447.44
10876.06
BV
18
17.31

744919.94
19933.02
W
19
18.27

587216.38
12229.08
VB
20
19.90

21970.00
880.00
BB
21
21.08 / ibe

716135.69
10977.59
BV
22
23.60

1.08e6
23242.34
VB
23
25.61 Q6
-------
25	32.82	146959.91 2116.02 BV
26	35.08	339117.00 4874.37 W
27	39.90	289010.50 919.72 VB
Total Area « 9124248.00
REPORT BY TIM RAND, LOCKHEED-ESC

000224

-------
Fileilaae : e:\pkd\HCFR012.rau	Oate: 8/J0/89 12:16 PN Page 1 of 1	^
Start Viae: 0.00 ain End liie: 47.00 ain Low Point: 5*20 uV High Point: 90250 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 tU Plot Scale: 60 mV
Qj
cr>
CO
<3_>
ct;
60.000-
50.000-
40.000-
30.000-
20.000-
10.000-
0.000-
o
o
o
t\i
N
CI
in ^GO m
""1 **2 ^
—* ix«j nS «d ^	V jri h» t7>
(«<-> r— io
»»"» V I—*
CNi DO
»»"» vr>
3

<=n
r^Tl
23 . 50
39. 17
I I I I I | I I I I I I I I I 1 I I 1 I I
7.83	15.67

-------
Nelson Analytical 2700 chromatography System Report Header
Sample Name : AXU.221
Sample Number: PCB1221
operator : tar
Time
Study
8/30/89 12:18 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : s A/D aV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 ain.
End Time	: 47.00 rain.
Sampling Rate : 1.0 pts/sec
8:29 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0i3.raw
e:\pkd\MCFR013.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 UL
1.0000 UL
Area Reject
100.00
********** PCB/TOXAPHENE STANDARDS REPORT *********
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Peak Ret Time Component
# [min] Name
Peak Area
[uV-sec]
Peak Ht
[UV]
BL
Type
1
1.42
61265.00
10416.36
BS
2
2.24
79357.56
9621.35
BV
3
2.55/^Z./
195860.80
21713.69
VB
4
3.30
26760.00
1778.28
BB
5
4.29
13440.00
1322.15
BB
6
9.05
5165.00
205.47
BB
7
13.03
8270.00
196.78
BB
8
14.43
7985.00
264.23
BB
9
21.14
148079.75
4252.91
BB
10
24.00
149847.38
3393.39
BV
11
25.61 Qi> C
1.13e6
25666.91
VB
Total Area - 1827843.25
REPORT BY TIM RAND, LOCKHIID-ESC
:ssssas»sssas
S3 C3BKBSSSS5 SS 33S IS
SSS5SSSSSSSSSSSSSS3SSSS3
000226

-------
Chromatoqrara
filed we : e:\pkd\MCfR01J.ran	Date: 8/30/B9 12:18 PH Page 1 of 1	3
Start Tiae: 0.00 ain End Tiae: 47.00 ain Lou Point: 4180 uV High Point: 11S520 uV
Vertical Scale factor: 0.00 Plot Offcet: 0 aW Plot Scale: 60 MV
60.000-
50.000-
40.000-
CL>
£5 30.000	
Q
CO

20.000-
10.000-
0.000-
o
o
O
ro
ro

WW-
in
to fO
•— -*r
C^l	CN CN
•j—-i-Trrr

T~r
i i i | i i i i i i i i i | i i i i
7.83	15.67
I I I | I I I I I I I I i | | i
23.50	31.33
I I I I I I
39. 17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Number:
Operator :
Interface # :
AutoSampler ;
Rack/Vial :
AS1232
PCB1232
tar
Time
Study
8/30/89 12:20 PM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time:	8/29/89
Delay Time : 0.00 min.
End Time : 47.00 min.
Sampling Rate ; 1.0	pts/sec
9:20 PM
Rav Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	.
Sample Amount	;
e:\pkd\MCFR014.raw
e:\pkd\MCFR014.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
100.00
3SSSS3SS
********** PCB/T0XAPHENE STANDARDS REPORT *********
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Peak
Ret Time
Component
Peak Area
Peak Ht
BL
#
[min]
Name
[uV-sec]
[uV]
Type
1
1.42

45250.00
6083.45
BB
2
2.23

44206.66
5809.77
BV
3"
2.55

146690.00
17316.64
VB
4
3.30

85410.00
8822.75
BB
5
3«84

33320.00
2644.87
BB
6
4.30/2*5 ~

153150.00
15077.42
BB
7
5.02

96200.00
3048.24
BB
8
6.36

79833.05
4489.99
BV
9
6.77

68784.34
3584.51
VB
10
7.47

37121.80
2279.89
BV
11
7.88

115623.84
5016.99
VB
12
9.13 >

85620.00
3548.55
BB
13
11.02

19164.17
501.15
BV
i4
11.70

18271.48
751.89
VB
15
13.05

22380.00
652.57
BB
16
15.76

13330.00
373.16
BB
17
21.14

189580.00
4703.71
BB
18
23.97

152323.50
3502.29
BV
19
25.57

1.17e6
26849.68
VB
000228
Total Area - 2579317.00

-------
REPORT BY TIM RAND, LOCKHEED-ESC
000229

-------
Chromatogram
FileNane : e:\pfcd\HCFROK.raw	Oate: 8/30/89 12:20 PM Page 1 of 1	7
Start Tine: 0.00 ain End Tiae: 47.00 Bin Low Point: 10 uV High Point: 91630 uV
Vertical Scale Factor: 0.00 Plot Offaet: 0 nv Plot Scale: 60 aV
CO

£9 30.000——
20.000-
10.000-
0.000-
i
Cs< ir»	co
3 3

5 S 5
CN	*N

-Art A
VtT°rT
—-rr
.	<<~tt
o
o
o
ro
^ri i i i i i i j i i i i i i i i i | i i i i i i i i i | i i i i
7.83	15.67	23.50
Time (min)
I
£z>
111 'pj 111111111 j 111111111
31.33
39. 17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1242
Sample Number: PCB-1242
Operator : tar
Time
Study
8/30/89 12:23 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time :	0.00 min.
End Time	:	47.00 min.
Sampling Rate :	1.0 pts/sec
10:12 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR015.raw
e:\pkd\MCFR015.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e: \pkd\pkdpcb. snip
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 100.00
PCB/TOXAPHENE STANDARDS REPORT
Instrument ID: Varian 3 400-1
GC Column ID: 2250/2401
Peak Ret Time Component
# [min] Name
Peak Area
[uV-sec]
Peak Ht
[UV]
BL
Type

.... !
1.55
13090.00
1. 00
BB

2
2.55
55480.00
6985.88
BB

3
3.31
78653.30
8341.17
BV

4
3.85
49700.20
3412.91
W

5
4. 3 0 / 2* V 1
181334.84
15728.82
VB

6
5.03
97569.94
2988.31
BB

7
6.36
78035.08
4391.47
BV

8
6.78
67054.63
3652.35
VB

9
7.47
37820.00
2370.63
BV

10
7.90
120290.00
5158.90
VB

11
9.15
88970.03
3645.36
BB

12
11.02
20648.30
539.38
BV

13
11.70
18893.52
767.21
VB

14
12.97
26750.00
829.93
BB

15
15.80
21160.00
576.09
BB

16
21.15
159590.00
4373.28
BB
000231
17
24.03
146121.88
3401.10
BV
18
25.63 Q4C
1.14e6
26008.06
VB

Total
Area = 2401225.00




REPORT BY TIM RAND, LOCKHEED-ESC

-------
000232

-------
FileNane : e:\pfcd\MCFR015.raw
Start Tine: 0.00 ain End Tim: 47.00 *in
Vertical Scale Factor: 0.00 Plot Offket:
«	Chroma tog ram
Oate: 8/30/89 12:23 PN	Page 1 of 1
Low P.iint: 3880 uV High Point: 175600 uV
0 UV Plot Scale: 60 nV
ro u> a in
S S S3 35 s
vr"»
60.000-
• • • • •
ro h~>
u=j
CN OvI
50.000-
40.000-

30.000-

CxZ
20.000-
10.000-
0.000-
"fT^T
•rr
O
O
O
rc
u-
CJ
I I I I
I I I I I I I
I I I I I I I I I I I I I I
7.83
15. 67
23 . 50
31.33
39 . 17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1248
Sample Number: PCB-1248
Operator : tar
Time
Study
8/30/89 12:25 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/29/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
11:03 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR016.raw
e:\pkd\MCFR016.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 100.00
PCB/TOXAPHENE STANDARDS REPORT
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Peak
#
Ret Time Component
[min] Name
Peak Area
[uV-sec]
Peak Ht
[UV]
BL
Type

1
1.55
10430.00
1. 00
BB

2
3.31
72947.79
7871.89
BV

3 .
3.78
53149.39
3455.80
W

4
4.30
292405.09
25192.52
W

5
4.71
150628.38
6309.37
W

6
5.44/1VS
299659.94
14405.98
VB

7
6.37
207240.44
12273.48
BV

8
6.79
212601.31
11391.48
VB

9
7.49
143854.73
8999.11
BV

10
7.91
479442.63
19075.98
W

11
9.16
364400.50
14000.70
VB

12
11.07
117180.41
2857.69
BV

13
11.72
100902.56
3897.18
VB

14
13.07
146360.00
4591.77
BB

15
14.43
27915.00
857.86
BB

16
15.82
108120.00
3253.83
BB

17
17.47
30551.10
926.27
BV

18
21.33
163670.88
4316.37
VB
Q00234
19
24.17
181006.00
3642.78
BV
20
25.84
1.17e6
26259.75
VB

Total Area = 4333220.00

-------
REPORT BY TIM RAND, LOCKHEED-ESC
000235

-------
Filename : e:\pkd\MCFR016.rau	Date: 8/30/89 12:25 PH Page 1 of 1
Start Tiae: 0.00 ain End Tiae: 47.00 ain Lou Point: 490 uV High Point: 88100 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 60 101
ii"i ^~— ' <"•>»	r-^ r^> cvi r-^

£
CO

60.000
SO.000
40.000
30.000
20.000
10.000
0.000
7.83
15. 67
23.50
Time (min)
i
I l i *P| I I I I l I I l I | I I I i l I I l l
31.33
39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : AR1254
Sample Number: PCB-1254
Operator : tar
Time
Study
8/30/89 12:27 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
2S5/2S5
10000
Data Acquisition Time: 8/29/89
Delay Time : o.oo min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
11:56 PM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR017.raw
e:\pkd\MCFR017.rst
e:\pkd\pkdpcb.ins
e:\pkd\pkdpcb.pre
e:\pkd\pkdpcb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 100.00
********** PCB/TOXAPH1N1 STANDARDS REPORT *********
—Tffi'SagtggS'gg'S—<11. iiiiiaaiwga»cgn'"'iisi!3aaggs*y

660939.63
19355.64
W
10
14.38

377089.09
10080.90
VB
11
15.79

408694.97
11615.29
BV
12
17.37

598106.19
15350.61
VI
13
18.35

42730.00
1240.43
IB
14
19.55

14125.00
551.21
BB
15
21.17

288032.59
5251.17
BV
16
22.52

117935.81
2805.84
W
17
23.99

246120.92
4186.82
w
18
25.68

1.15e6
26299.70
VB
19
27.83

66630.00
1560.30
BB

Total Area = 5516259.50
:ssssaas!

-------
REPORT BY TIM RAND, LOCKHEED-ESC
000238

-------
Chromatoqram
fileName : e:\pkd\MCM017.raw	Date: 8/30/89 12:27 PM Page 1 of 1
Start Tine: 0.00 ain End Tine: 47.00 Bin Lou Point: 1010 uV High Point: 91930 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 60 art/
Lt-a
s
cu
cr>
co
a>
CXL
60.000-
50.000-
40.000-
30.000-
20.000-
10.000-
0.floo-
rs u-> on	lt> aa av	u~>	pm	cn	ao
23	S ^	SO	"3	53	23
cj	»*"» -it irt	cH	«— 
-------
Nelson Analytical 2700 chromatography System Report Header
Sample Name
Sample Number
Operator
Interface #
AutoSampler
Rack/vial
EVALB
Time
Study
8/31/89 2:12 PM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
5:06 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR02 3.raw
e:\pkd\MCFR0 2 3.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
kEXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlma Cooponant Adjuatad Amount Saw Amount	Paak Araa	Paak He	MULTIPLIER
(mini Kama	UC/L	UC/L	[uV-«ae|	(uVl	AdJ/Raw
5.20 ALDRIN	0.00	0.00	1.33a6	100196.98		
10.87 DDE	0.00	0.00	10743.00	400.00		
13.17 ENDRIH	0.00	0.00	783768.69	27906.37		
13.31 DDD	0.00	0.00 63760.00	1769.21		
17.37 DDT	0.00	0.00 *81167.38	12381.86 	
23.39 DBC	0.00	0.00 748818.00	16610.87		
Total Araa - 14277*4.30
Total Cooeancratlon - 1.0000
Report by Tim Rand, Lockheed-ESC
000240

-------
Chromatoqram
Filettane : e:\pfcd\HCFR023.rau	Date: 8/31/89 2:13 PN Page 1 of 1	^
Start Tfae: 0.00 ain End Tiae: 47.00 ain Low Point: 3250 uV High Point: 2KJ40 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 250 mV
a>
£>~>
o
CO
o_>
o;
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
O
o
o
in
K

L-
n
I I I I I
=2L
r- in u->
mS r-^
orv	<—> crv
i-	o in
•	»	_•
•—	T	if»
rJUr rArrr^rr-A
I	I " I I
I I I
^ H ^ s s
Is? I i*Y I P| I Pi *T
i i i i i I i ii i
7.83
15 . 67
23 . 50
I I I I | I I I I I I I I I | I I I I I I I I I
31.33	39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : INDA
Sample Number: 100/200A
Operator :
Time
Study
8/30/89 11:12 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D raV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time:	8/30/89
Delay Time : 0.00 min.
End Time : 32.75 min.
Sampling Rate : 1.0	pts/sec
10:15 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR029.raw
e:\pkd\MCFR02 9.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0. 00
kEXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
R«C T1m
(min)
Cooponant
Adjuatad Amount Riw Aoount Peak Aria P«ak Be MULTIPLIER
UC/L	UC/L (uV-a«e) [uVJ Adj/Rav
3.33
G-BHC
10S.79
106.79
2.30*6
278088.81
1.00
4.13
HPTC9LR
108.76
108.76
2.36«6
210721.09
1.00
3.22
AL0RIN
103.97
103.97
2.43*6
182082.92
1.00
7.68
HEPEPOX
106.43
106.43
2.16*6
114827.64
1.00
9. *3
EHD01
106.00
106.00
2.04*6
90476.07
1.00
11.23
DIttDRIH
212.67
212.67
4.60*6
179601.03
1.00
13. *2
END02
214.74
214.74
6.02*6
180291.41
1.00
17.41
DOT
212.77
212.77
1.81*6
33008.00
1.00
18.SI
ENDAL0
211.31
211.31
2.77*6
37361.23
1.00
23.66
DBC
206.63
206.63
2.73*6
60163.62
1.00
27.03
MEIBOCX
1026.22
1026.22
3.40*6
123239.86
1.00
Total Araa ¦ 3*909869.00
Total Concentration • 2618.3032
y
Report by Tim Rand, Lockheed-ESC
000242

-------
Chromatogram
FileNane : e:\pfcd\HCFR029.raw	Date: 8/30/89 11:13 AM Page 1 of 1
Start Tine: 0.00 ain End Km: 32.75 «fn Lou Point: 3400 uV High Point: 279730 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 DV Plot Scale: 250 ntv
hO
OJ
f>0 CN
5a
250.000-
u—> oa
*—
vrt
fx od
U> IT*	CN
CN
i	_? _ r
T ¦/>
«N CN
Qj
CO
o_»
Ck£
208.333-
166.667-
125.000-
aj.ju-
41.667-
-0.000-
~fr—iy\V;

UUUUV1
II .	M »	I <	I	II
©
o
o
10
CJ
TT
<-> 2
i i F*! i i i *f* i i 'r 'i i i i i i i i V 'i | i *Pi l'f i i i i | • i i » " > T"i i "| i i i i i i i i "
hi
&

5.46
10.92
16. 38
21.83
27.29

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : INDA
Sample Number: 100/200A
Operator :
Time
Study
8/30/89 11:12 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 32.75 min.
Sampling Rate : 1.0 pts/sec
10:15 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR029.raw
e:\pkd\MCFR029.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
tEXTERNAL STANDARD REPORT*
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tlaa
Cooponant
Adjiucad Amount Raw Amount Peak Araa
P*ak Bt
MULTIPLIER
[mini
Nam
UC/L
UC/L
(uV-i.c)
[uV]
AdJ/Raw
3.53
C-BHC
106.79
106.79
2.50.6
278088.81
1.00
4.33
HPTCSLR
108.76
108.76
2.36*6
210721.09
1.00
5.22
AL0RIH
103.97
103.97
2.45*4
182082.92
1.00
7.68
HEPEFOX
106.43
106.43
2.16*6
114827.64
l. 00
9 .4*1
END01
106.00
106.00
2.04*6
90476.07
1.00
11.23
0IELDRIH
212.67
212.67
4.60*6
179601.01
1.00
13.42
E8D02
214.74
214.74
6.02*6
180291.41
1.00
17.61
001
212.77
212.77
1.81*6
51008.00
1.00
18.81
EH0ALD
211.11
211.11
2.77*8
37161.23
1.00
23.66
0BC
206.61
206.61
2.73*6
60163.62
1.00
27.03
METHOXY
1026.22
1026.22
5.40*6
123239.86
1.00
Total Azaa - 14909868.00
Total Concentration - 2618.1092
Report by Tim Randf Lockheed-ESC
000242

-------
Chromatogram
FileMane : e:\pkd\MCFR029.ran	Date: 6/30/69 11:13 AH Page 1 of 1
Start line: 0.00 ain End liM: 32.75 sin Low Point: 3400 uV High Point; 279730 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 mV
 oca
Cn	~—
~ r-S

co oa
cd
u> u-»
vT>
CN CN
TT

cr»
CN
i T^i i i n H i
21.83
5.46
10.92
16. 38
27.29

-------
Nelson Analytical 2700 Chromatography System Report Header
I
lample Name
Sample Number
operator
interface #
AutoSampler
Rack/Vial
EVALB
Time
Study
8/31/89 2:15 PM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Jata Acquisition Time: 8/30/89
Delay Time : 0.00 min.
"?nd Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
4:28 PM
Raw Data File	:
lesult File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 3 5.raw
e:\pkd\MCFR035.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\pkdeval.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00


* * * * * EXTERNAL STANDARD
REPORT*****

Instrument ID:
Varian 3400-1 GC Column
ID: 2250/2401

fl'.at Tina
[mini
Caopenanc
Adjuatad Amount Raw Amount Paak Araa Peak Ht
UG/L UC/L [uV-iael [uV]
MULTIPLIER
Adj/Rav

3.20
ALDRIN
0.00
0.00
1.46a6
109938.22
13.19
ENDRIN
0.00
0.00
811320.00
30979.37
13.33
ODD
0.00
0.00
193030.00
3033.73
17.39
DOT
0.00
0.00
320313.00
9690.92
23. «2
DBC
0.00
0.00
804673.13
18182.20
Tool Aria ¦ 1391833.30
Total Concentration ¦ 1.0000
Report by Tim Rand, Lockheed-ESC
000244

-------
FileNane : e:\pkd\HCFR035.raw	Oate: 8/31/89 2:15 PM Page 1 of 1
Start Tine: 0.00 «in End liw: 47.00 ain Low Point: 4560 uV High Point: 208630 UV
Vertical Scale Factor: 0.00 Plot Offset: 0 Plot Scale: 250 mV
u-»
"1

CxZ
250.000-
208.333-
166.667-
125.000-
83.333-
id
crt r~r~) cn
*— m lr>
•*"» m~5 r-
r
41.667-
-0.000


KT
, ,r, , ,
r
-------
Nelson Analytical 2700 Chromatography System Report Header
ample Name :
Sample Number:
Operator
interface #
AutoSampler
lack/Vial
INDB
100/200B
Time
Study
8/31/89 12:52 AM
MCFARLAND
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
oata Acquisition Time: 8/31/89
pelay Time : 0.00 min.
!nd Time	: 35.03 min.
iampling Rate : 1.0 pts/sec
12:15 AM
Raw Data File	:
| tesult File	:
.instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR04la.raw
e:\pkd\MCFR04la.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
~~~~~EXTERNAL STANDARD REPORT*****
instrument ID:
Varian 3400-1

GC Column
ID: 2250/2401
¦t Tla* Coaponant
MJuacid Amount Raw Amount ?*ak Araa
?*ak Ht
MULTIPUHl
(mini tlaaa
US/L
US/L
[uV-s*c|
[uV]
Adj/fUv
2.77 A-BBC
116.41
116.41
3.46*6
320271.aa
1.00
<>.08 1-BHC
114.04
114.04
1.02*6
94974.12
1.00
4.74 D-BHC
116.64
116.64
2.48*6
213025.41
1.00
5.23 ALDUS
110.37
110.37
2.74*6
206376.38
I. 00
a.49 C-CHLDAHX
110.35
110.33
2.29*6
114205.22
1.00
9.21 A-C8L0A8Z
108.78
108.78
2.28*6
103783.48
1.00
10.87 DDI
220.44
220.44
4.40*6
183093.69
:.oo
13.23 rami*
203.31
203.31
2.82*6
99567.81
1.00
15.33 ODD
230.90
230.90
3.56*6
110140.44
1.00
21.43 EHDOSULTATX
221.20
221.20
1.99*6
46369.36
1 30
23.74 DBC
263.73
263.73
2.94*6
74239.28
:.oo
26.24 U1IU1IJ
188.60
188.60
3.03*6
73963.03
1.00
Total Ana - 33077338.00
jfotal Concentration ¦ 2005.1608
Report by Tim Rand, Lockheed-ESC
h
000246

-------
Response (uV)
ifrZOOO
ihihiiIiiiiiihiIhiiiiii
ill in ii in ill in	1
mw:
-3-BHC
-FLORIN
:3-CH LQANE
ict
[NORIW
tico

f
=L
: 1.09
- 2.77
: i?3
•	M
•	W
•	10.B7
•ii?3
•	1133
::nkmfai[
-)EC
-18.56
-	21.0
• 24.07
-	2176
27.96

-------
Nelson Analytical 2?00 Chromatography System Report Header
ample Name : INDA
sample Number: 100/200A
Operator :
Time
Study
8/31/89 12:25 PM
MCFARLAND
nterface #
AUtoSampler
jtack/Vial
: 2	channel : B a/D mV Range
: Varian 8000 without controller
: 255/255
10000
ata Acquisition Time: 8/31/89
Delay Time : 0.00 min.
*nd Time	: 47,00 min.
ampling Rate : 1.0 pts/sec
8:38 AH
Raw Data File
esult File'
nstrument File
Process File
Sample File
"equence File
Inj. Volume
¦Sample Amount
e:\pkd\MCFR04 3.raw
e:\pkd\MCFR0 4 3.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
asa—juaasaas
sasssss
~EXTERNAL STANDARD REPORT*
nstrument ID: Varian 3400-1
GC Column ID: 2250/2401
1*1 IIam
(min)
CoapoaasE
AdjuJCKd Aaoixax. Staw Amount F**k An*
US/L	mi [uV-««e)
P«*k Be
[uVJ
KUITXH.XER
Adj/Rsv
3.3*
4.34
S.22
7.69
9,43
11.26
13.42
17.62
18.82
as.jo
27.10
G-SBC
HPTCHT.B
AUKIH
HEPEPOX
EHD01
DlttDRIB
EHD02
DDT
OISALD
DBC
1U.89
ItS.10
106.06
105.59
10*.8*
207.8*
202.43
274.93
214.48
206.34
1186.16
111.89
113.10
108.06
103.39
104.64
207.8*
202.43
274.93
214.48
206.34
1188.16
2.62*6
2.49*6
2.43*6
2.14*6
2.01*6
4.49*6
3.67*6
2.13*6
2.81*6
2.73*6
6.23*6
307318.97
231041.13-
188993.38
117871.97
92332.76
181328.36
178634.41
69639.20
60860.88
61913.21
145803.72
.00
.00
.00
.00
00
00
00
00
00
00
00
ockl Ar«» - 16090736.00
ot*l Concmtriclon - 2833.6*33
¦toport by Tim Rand, Lockheed-ESC
000248

-------
\	„ ,	Chromatogram
FileNrae : e:\pkd\MCFRCK3.raw	Date: 8/31/89 12:25 PH Page 1 of 1
Start Tiae: 0.00 afn End Tiae: 47.00 ain Lom Point: 9270 uV High Point: 317260 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 »V Plot Scale: 2S0 mV
-— CN	(O
cri -f
io	cn
CO
r-*
Q_>
cr>
CO
(L)
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
L
fnf

Tf
I
r
iii	i i i
t in rv o
<->>4 CN CN CM
c
o
o
10
(X)
39. 17
23.50
lb . 67
7 .83

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
pmple Number
erator
EVALA
T ime
Study
8/28/89 10145 AM
MCFARLAND
iter-face #
;toSampler
ck/Vial
5
None
0/0
Channel
attached
A/D mV Range : 1000
ftftta Acquisition
lay Time
e" d Time
Sampling Rate
w Data File :
F~.suIt File :
instrument Files
ocess File
mp1e File
Sequence File
tj. Volume
mple Amount
Timet
0.00
70.00
1.0
8/28/89
min.
min.
pts/sec
8109 AM
C:\2700\GC3\MCF3002. raw
C:\2700\GC3\MCF3002.rst
C:\2700\GC3\F0E.ins
C!\2700\GC3\EXSTD.pre
C:\2700\GC3\MCCEVAL.smp
C:\2700\GC3\MCF34A. seq
2 uL
1.0000
Area Reject
: 0.00
^3ise Threshold:
lution Factors
visor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
1.00
0.00
Bunch Factor:
istrument Conditions:
pi liary GC -
Instrument	:VARIAN
Column	:	.23MM
Column Length	:	30M
Carrier Gas	:	HE
Flow Rate	:	20CM/SEC
Split Ratio	:
Temperature	:	160
Injection Temp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400
ID .2SUMFILM RTX5
LINEAR VELOCITY 15" PS I
1/MIN TO 230
Total Number o-f Peaks Detected! 18
.»at Time
Cmin]
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L	CuV-sec3
Peak Ht
CuV3
Raw Amount
ug\L
1.62
1.81
3.69
12.37
21.34 ALDRIN
30.48
000250
3783.02
44434.30
787.00
486.30
0.00
02.50
11370.03
88308.39
1374.00
973.00
43177.02
403.00
4433.36
3192.76
16.82
34.77
2963.23
31.32
5785.02
44154.30
787.00
486.50
0.00
202.30

-------
36.71 ENDRIN	0.00	10861.00
38.19	365.50	731.00
41.05 DDD	0.00	1769.00
44.09	1592.00	3184.00
46.01 DDT	0.00	15612.00
51.24 ENDKETO	0.00	604.50
54.31	633.75	1267.50
55.93	961.501923.00
60.15	318.50	-
61. o3 DBC	0. 00
64.34	682.75	1365.50
65.86	483.50	967.00
S66.29
0. 00
57.03
365.50
155.o2
0.00
270.39
1592.00
1362.35
0.00
52. 48
0.00
108.07
633.75
115.84
961.50
62.26
318.50
•944.48
0.00
113. 15
682.75
86.27
483.50
Total Area = 197462.16
Total Concentration = 56452.8164
Report by Doherty Bresnahan
000251

-------
FileNaw t C:\Z700\6C3\»CF3002.rw	Oatai 8/2B/89 10t4S All Pag* 1 of 1
Start Tiatt 0.00 ain End Tiaa» 70.00 ain Lot Pointi 4927 uV High Pointi 9550 uV
Vertical Scale Factor« 0.00 Plot Offwti 0 aV Plot Scalai 100 aV
Chiaaatograi
> a
UUH
0J8-;
IShi
- * « * -
ill ; ::
*	!S KS
a »B ii si
JMH
aar
HW-t
nih-
il n ii ii ii fi nci mi ii
t«
111
liw
J .
a ¦ a
* I ' '
23.0
¦ 111
3.33
3S.0I
TIm (lin)
1H.il
000252

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
EVALB
T ime
Study
8/20/89 10!47 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
O/O
A/D mV Range : lOOO
Data Acquisition Times 8/28/89 9:23 AM
De 1 ay T i me	:	0. 00 m i n.
End Time	:	70.00 mm.
Sampling Rate :	1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5003.raw
C:\2700\GC5\MCF5003.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCCEVAL.smp
C:\2700\GC5\MCF54A-seq
Inj. Volume
Sample Amount
2 uL
1. 0000
Area Reject
o. 00
Noise Threshold: 1
Dilution Factor: 1.00
Divisor	: 1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
1.00
0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .2SUMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 14
Ret Time
Cmin D
Componen t
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L	CuV-sec3
Peak Ht
CuV]
Raw Amount
ug\L
1.62
1.83
3.73
21.55 ALDRIN
24.65
34.62 DDE
1888.39
12233.56
3776.78
24467.11
9672.03
08708.50
625.50 1251.00
0.00 1134.00
000233;::»20i
1106.85
942.58
50.95
131wO.58
98.00
73.58
isse.3?
12233.56
4936.02
0. 0<
625. 5<
0. 0<

-------
36.74 ENDRIN
40.79
41. 13 DDD
46.05 DDT
48.38
51.28 ENDKETO
60.21
61.37 DBC
0.00
766.34
0.00
0.00
269.50
0.00
1458.00
0.00
50453.00
1532.69
1893.44
63466.98
539.00
3090.00
2916.00
44098.00
4049.02
76.71
137.32
5601.20
41.66
254.53
279.92
4034.73
0. 00
766.34
0.00
0.00
269.50
0.00
1458.00
0.00
1_tal Area = 417000.56
Total Concentration = 22077.3047
Bpport by Doherty Bresnahan
000254

-------
FileNaaa : C:\2700\GC5VCF3003.Ptt	Date: 8/28/09 10:48 AH Page 1 of 1
Start TiM< 0.00 ain End Tine* 70.00 ain Lm Point) 4911 uV High Point: 13240 uV
Vertical Scala Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Chrciatogra*
C.JB-

m
I
A
U.W
23.33
35.00
Tiie (us)

58.33
000255

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
Inter-face #
AutoSampler
Rack/Vial
EVALC
5	Channel
None attached
0/0
Time
Study
8/28/89 11:55 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition Time« 8/28/89 10:37 AM
Delay Time	: 0.00 min.
End Time	: 70.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File :
Result File :
Instrument File>
Process File :
Sample File :
Sequence File
C:\2700\GC3\MCF5004.raw
C:\2700\GC5\MCFS004A.rst
C:\2700\GC3\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCCEVAL.smp
C:\2700\GC5\MCF54A.seq
Inj. Volume :	2 uL
Samp 1e Amoun t :	1.0000
Noise Threshold:	1
Dilution Factors	1.00
Divisor	:	1.0000
Area Reject
Area Threshold
Mult ip1ier
Additive Constant
0.00
100
1.00
0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Spirt Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PSI
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected: 17
Ret Time
Cmin]
Componen t
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L	CuV-sec3
*********
Peak Ht
CuV3
Raw Amount
ug\L
1.62
1.80
3.55
J1.49 ALDRIN
24. 61
54.58 DDE
5614.23
40711.41
3781.00
11228.46
81422.83
7362.00
0.00 387716.50
Q00256
1599.00
0. 00
3198.00
2258.00
4751.32
2962.49
54.98
22815.53
193.06
138.91
5614.23
40711.41
3781.00
0.00
1599.00
0.00

-------
36. 70
ENDRIN
0.00
92654.00
7056.73
0.00
40.76

1508.21
3016.42
144.35
1508.21
41.11
DDD
0.00
3266.55
245.01
0.00
46.05
DDT
0.00
121951.50
10624.09
0.00
50.66

278.00
556.00
47.33
278.00
51.29
ENDKET0
0.00
6441.00
527.38
0.00
53. 08

315.50
631.00
55. 11
315.50
56.58

315.00
629.99
52.92
315.00
60.24

2943.46
5886.92
528.54
2943.46
60.72

3820.82
7641.64
345.49
3820.82
61.40
DBC
0.00
81798.00
7558.70
0.00
Total Area = 817858.31
Total Concentration = 60886.6328
Report by Dohertv Bresnahan
000257

-------
FiltNaw : C:\2700\6C3\MCF3004.ru	Datat 8/28/89 11:36 AN Pa$a 1 of 1
Start Tiae« 0.00 ain End Tiaai 70.00 ain Lom Points 4942 uV High Pointi 27922 uV
Vertical Seals Factor! 0.00 Plot Offwti 0 «V Plot Seals* 100 aV
Chroutograa
3J.M
Tilt (tin)
000258

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :
Sample Numbers
Operator	s
100/200 A
Time
Study
8/29/89 a:47 AM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
5	Channel
None attached
O/O
A/D mM Rang*
1000
Data Acquisition Timet 8/28/89
Delay Time i 0,00 min.
End Time	: 70,00 min.
Sampling Rate : 1.0 pts/sec
II PM
Raw Data File
Result File
C:\2700\GC5\MCF5007. raw
C!\2700\SC5\MCF3007B. rst
Instrument File! Cs\2700\GC5\FOE.ins
Process File
Sample File
Sequence File
CJ\2700\GC5\EXSTD. pre
Cs\2700\GC5\MCF51 A. smp
Cs\2700\GC5\MCF54A. seq
In ,j. Volume
Sample Amount
2 uL
1.0000 UG/kq
Area Reject
: 0.00
Noise Thresholds 1
Dilution Factors 1.00
Divisor	: 1.0000
Area Threshold '• 100
Mu 11 i p1i er	: 1. 00
Additive Constants 0.00
Bunch Factors 1
Instrument Conditions!
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
In j ec t i on Temp
Detector 1
Detector 2
Notes
3400
ID .25UMFILM RTXJ
sMARIAN
s .25MM
30M
HE
20CM/SEC LINEAR VELOCITY IS
160 1/MIN TO 230
200
300
PSI
Total Number of Peaks Detected! 30
********** EXTERNAL STANDARD REPORT
Ret Time
CminJ
Component
Name
Adjusted Amount Peak Area
uq\L	CuV-sec J
tftft******
Peak Ht
CuV]
Raw Amount
uq\L
1
58
G-BHC
18.12 HPTCHLR
21.47 ALDRIN
26.05 HEPEPQX
30.37 END01
33.82 DIELDRIN
000259
100.00 403396.00
100.00 193774.50
100.00 429065,00
100.00 280921.00
100.00 263714.13
200.00 284475.13
23713.33
10687.36
27670.81
19015.28
18518.12
21516.71
100.00
100.00
100.00
100.00
i 00.00
200.00

-------
38.11 END02
40.99 ENDALD
43.97 DDT
53.94 METHOXY
¦ 61•DBC
200.00	457726.00
200.00	188465.50
200.00	314350.25
1000.00	369524.00
200.00	192333.00
35802.02
14856.85
27228.23
33898.45
17875.01
200.00
200.00
200.00
1000.00
200.00
. al Area - 3377744.50
"ocal Concentration = 2500.0000
Report by Doharty Bresnahan
000260

-------
FileMiM : C:\2700\GC3\nCF5007.raM	Date: 8/29/89 8:48 Ml Page I of I
Start Tine: 0.00 «in End Tiae> 70.00 ain Low Point) 4991 uV High Point: 40878 uV
Vertical Scala Factor: 0.00 Plot Offset: 0 nV Plot Seals: 100 aV
Ckrautograi
SS 33s:
si ii mm
55* ft KM

m
I
¦m
23.33
8.00
Til* (lin)
0002G1

-------
Nelson Analytical 2700 Chromatography System Report Header
nple Name :
Imp la Numberi
orator	:
100/200 B
Time
Study
9/29/99 8:2:
MCFARLAND
AM
[ufcer-face #
iBtoSampler
»:k/Vial
5	Channel
Nona attached
0/0
A/0 mV Range : 1000
Data Acquisition Timet 8/28/89
I lay Time	: 0.00 min.
d Time	> 70.00 min.
3 npling Rate : 1.0 pts/sec
4i43 PM
4|w Data File
Vault File
I atrument File:
||ocess File
»nple File
Pquence File
C:\2700\GC3\MCF3008.raw
C:\2700\GCS\MCF3008.rst
C:\2700\GCS\F0E.ins
C:\2700\GC3\EXSTD.pre
C:\2700\GC3\MCF31B. smp
C:\2700\GC5\MCF54A.ses
1
j. Volume
nple Amount
2 uL
1.0000 UG/kg
Area Reject
: 0.00
^Joise Threshold: 1
Ilution Factor: 1.00
visor	: 1.0000
Area Threshold
Mu 11 i p1i er
Additive Constant
100
1.00
0.00
Bunch Factor!
1
strument Conditions:
Pi liary GC -
Instrument	JVARIAN
Column	: .23MM
Column Length	'• 30M
Carrier Gas	J HE
Flow Rate	: 20CM/SEC
Split Ratio	:
Temperature	: 160
I n j ec t i on T emp. : 200
Detector 1	: 300
Detector 2	:
Notes	:
3400
ID .25UMFILM
RTX3
LINEAR VELOCITY 15 FSI
1/MIN TO 230
1. tal Number of Peaks Detected: 29
Ft Time
.min]

Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L	CuV-sec]
Peak Ht
CuV]
Raw Amount
ug\L
10.31 A-BHC
11.98	B-BHC
14.IS D-BHC
21.51 ALDRIN
28.99	G-CHLDANE
30.95 A-CHLDANE
000262
100.00 462939.00
100.00 136307.00
100.00 347346.00
100.00 404708.00
100.00 337136.16
100.00 339307.94
23814.83
8792.30
21337.44
26177.13
23012.71
23824.02
100.00
100.00
100.00
100.00
100.00
100.00

-------
34.54 DDE
36.68 ENDRIN
40.47 DDD
44.59 ENDOSULFATE
51.22 ENDKETO
61.35 DBC
200.00 593944.00
200.00 174980.00
200.00 211850.30
200.00 363798.50
200.00 206602.00
200.00 151393.00
48390.96
13736.97
17901.48
27975.96
16834.00
14051.65
200.00
200.00
200.00
200.00
200.00
200.00
Total Area = 3750711.75
Total Concentration = 1800.0000
Report by Doherty Bresnahan
000263

-------
leNut : C:\2700\GC5\nCF500e.rw	Date: 8/29/89 5:22 AH Pap 1 
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
TOX
T ime
Study
8/29/89 8:26 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Times 8/28/89 5s!
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
70.00
1.0
min.
min.
pts/sec
C s\2700\GC5\MCF5009.raw
C:\2700\GC5\MCF5009.rst
C:\2700\GC5 \FOE.ins
C:\2700\GC5\EXSTD.pre
C:\27G0\GC5\MC5T0X.smp'
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
Multiplier
Additive Constant
100
1.00
0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument	JVARIAN
Column	:	. 23MM
Column Length	:	30M
Carrier Gas	:	HE
Flow Pate	:	20CM/SEC
Sp1i t Ratio	:
Temperature	:	160
Injection Temp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400
ID .25UMFILM
RTX5
LINEAR VELOCITY 13 PS I
1/MIN TO 230
Total Number o-f Peaks Detected: 64
Ret Time
Cmin ]
Component
Name
EXTERNAL STANDARD REPORT ****"—
Adjusted Amount Peak Area Peak Ht
ug\L	CuV-sec] CuV]
Raw Amount
ug \L
1.62
1.79
10.25
13.-01
21.23
23.49
000265
112421.69
704886.63
151.00
121.50
4211.75
522.00
224843.38
1.40e6
302.00
243.00
3423.50
1044.00
S6595.30
48579.13
33.95
23.67
461.93
44.87
112421.69
704886.63
151.00
121.50
4211.75
522.00

-------
27.
29.
30.
30.
31.
34.
34.
35.
36.
36.
37.
38.
3a.
39.
39.
40.
40.
41.
41 .
42.
42.
43.
44.
45.
45.
46.
47.
48.
48.
49.
49.
49.
50.
50.
51.
52.
52.
53.
54.
55.
55.
56.
57.
57.
58.
58.
59.
59.
60.
60.
61.
62.
62.
68.
63
86
19
27
62
95
03
39
74
54
85
20
19
71
42
08
89
61
89
55
90
53 -TeXAPHENE
86
63
11
40
•J -J
83
55
63
46
77
15
55
93
64
96
90
28
86
45
72
56
91
65
14
68
09
69
53
14
81
32
52 •
90
90
DDC P&
0002GB
2397.00
4794.00
243.44
2397.00
855.00
1710.00
168.81
855.00
998.25
1996.50
123.48
998.25
395.49
790.98
77. 42
395.49
947.94
1895.88
138.27
947.94
166.50
3 c* w .00
30.94
166.50
779.54
1559.07
137.98
779.54
3679.59
7359. 19
492.37
3679.59
2624.14
5248.28
319.13
2624.14
258.25
516.50
51.33
258.25
397.25
794.50
105.33
397.25
591.00
1182.00
118.50
591.00
3932.21
7864.42
460.90
3932.21
6290.95
12581.91
740.24
6290.95
726.50
1453.00
61.05
726.50
4267.49
8534.98
581.28
4267.49
2631.50
5263.00
305.36
2631.50
1835.66
3671.33
357.93
1835.66
6354.66
12709.33
833.17
6354.66
3670.75
7341.50
504.12
3670.75
3407.25
6814.50
379.00
3407.25
0.00
1196.97
86. 63
0.00
1394.64
2789.28
180.47
1394.64
1115.19
2230.38
160.36
1115.19
2705.64
5411.28
413.09
2705.64
2233.50
4467.00
298.63
2233.50
5461.50
10923.00
605.58
5461.50
7719.23
15438.45
1181.93
7719.23
7227.75
14455.50
909.65
7227.75
3502.50
7005.00
493.96
3502.50
1404.00
2808.00
250.67
1404. (50
974.40
1948.79
177.60
974.40
1358.93
2717.87
179.09
1358.93
990.40
1980.80
209.59
990.40
6146.45
12292.89
563.72
6146.45
5068.38
10136.75
681.94
5068.38
7895.98
15791.97
1148.69
7095.98
974.00
1948.00
181.81
974.00
5559.72
11119.44
. 651.29
5559.72
2062.29
4124.58
3-w-j .84
2062.29
891.50
1783.00
172.50
891.50
3133.00
6266.00
281.02
¦j 1 -i>o ¦ 00
5534.50
11069.00
567.98
5534.50
1772.73
3345.47
269.39
1772.73
1442.62
2885.23
196.18
1442.62
1334.76
2669.52
201.63
1334.76
403.72
807.44
59.20
403.72
3781.64
7563.28
611.18
3781.64
663.07
1326.14
116.40
663.07
908.50
1817.00
170.72
908.50
1088.16
2176.33
194.69
1088.16
837.57
1675.13
149.65
837.57
2584.49
5168.98
433.48
2584.49
1686.00
3372.00
271.80
1686.00
39529.50
77039.00
7254.71
39529.50
0. 00
704.75
57.55
0.00
144.93
289.86
31.98
144.93
146.00
292.00
23.08
146.00
Total Area
2000299.00


-------
Total Concentration = 999198.6230
Report by Doherty Bresnahan
000267

-------
I' fteaa : C:\2700\GC3\ICF5009.ru	Ditas 8/29/89 8:27 AH Pag* 1 ofl
t Tiwi 0.00 tin End Tia*i 70.00 ain Low Point' S132 uV High Point' 91844 uV
lbkicil Scale Fictori 0.00 Plot Offsets 0 aV Plot Scalai 100 aV
Chxaiatograa
1MH
OSH
CU9-E
swH
is.so-3
ii
TT
3 t 3	a
K C B	#;C35 C r»a BMBkllllB I
ii ii ii urn i miuTirmrmii'iTrimrrrrm'uTiifniih in
T~
SB.33
11(7
23.33
35.01
Tiu (lia)
«.<7
000268

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
PCB1660
Time
Study
9/29/89 9:30 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range i 1000
Data Acquisition Timet
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
70.00
1.0
9/2B/B9
min.
min.
pts/sec
7:14 PM
C:\2700\GCS\MCF5010.raw
C:\2700\GC5\MCF5010.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCC1660.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
s i). 00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold
flu 11 i p 1 i er
Additive Constant
100
1.00
0.00
Sunch Factor! 1
Instrument Conditions:
Cap i1lary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sp1i t Rat io
T emperature
I n j ec t i on T emp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 1!
PS I
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected! 79
EXTERNAL STANDARD REPORT
Ret Time	Component Adjusted Amount Peak Area Peak Ht	Raw Amount
Cmin]	Name ug\L CuV-sec] CuV]	ug\L
1.63	0.00 723783.75 248110.34	0.00
1.82	0.00 5.00e6 173345.42	0.00
0. 15	'J • 00 631.50 71 ¦	0.00
9.37	UUUfcUJ 0<00 3979.31 209.76	0.00
9.96	0.00 3748.14 267.29	0.00
10.30 PCB1016	242.14 27564.72 1292.75	242.14

-------
11.60
13.27
13.93
14.59
15.64
16.08
16.27
16.91
17.81
1 Q
iDi W4
19.01
19.80
20.29
20.72
21.08
21.29
22.46
22.77
23.79
24.71
25.42
26.08
26.52
27.01
"J7 CTT
tim i • vJy
nfl
«¦» o • *.o
29.50
79
30.	13
30.51
31.	16
33. 27
33.98
34.87
37.09
37.71
38.79
40.21
40.69
41.57
42. 44
44.27
45.50
46.45
46.80
47.85
48.66
49. 13
49.88
50.52
50.89
51. 41
52.66
53.46
54. 13
54.95
en
WW * SmO
56.	14
57.	14
mOI W
\ ^
x kr-
f

5°^
0	ci ^ *
fC>°
000270
P3
452.24
483.38
4780.62
2135.36
1638.75
433.08
129.74
1233.78
1159.08
1050.42
922.77
1674.58
1327.74
2106.84
486.79
65.04
68.73
423.85
660.24
1819.83
115.55
122.63
276.09
176.46
1801.35
66.79
109.77
555.80
672.86
1326.
2141.
1262.
4313.
290.33
105.23
1009.97
6259.05
2976.75
469.51
6415.12
1032.37
892.83
231.43
4519.14
2594.07
657.15
257.90
912.91
3797.70
2131.52
1330.66
142.82
303.71
900.36
10475.52
00
29
,90
,02
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0. 00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0. 00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00

-------
57.54

0. 00
7982.00
627.54
0.00
58. 16 PCD 1260 -Q&>
13.65
3015.47
255.33
13.65
58.83

0.00
4163.98
368.58
0.00
59.22

0.00
785.28
81. 18
0.00
60. 15

0.00
3221.00
307.17
0. 00
61.32



. 6687.04
73112.95
61.68

6184379^
~~ 6 lti4-.ii. V4
4596.90
61843.94
62.61-
-poc-o
0.00
1874.00
164.25
0.00
63. 19

26745.00
26745.00
2287.75
26745.00
64.02

32867.50
32867.50
2173.00
32867.50
66.39

1966.00
1966.00
175.89
1966.00
68.65

13676.00
13676.00
1081.90
13676.00
69.81

896.50
896.50
79.85
896.50
Total Area = 7265623.30
Total Concentration = 211363.6719
Report by Doherty Bresnahan
000271

-------
i C:\2700\H3\MCF3010.ran	Oatai 8/29/89 8:33 AN Pag« 1 of 1
Tiaat 0.00 ain End Tiaai 70.00 ain Lot Point* 5112 uV High Point: 253Z73 uV
/a icil Seal* Factor> 0.00 Plot Offset: 0 aV Plot Scalat 100 aV
Chrautograa
sa
«
1
4t
I
|MMt-
ojjH
5WH
asH
Kje-I
:;x stiefcu* cu »n«: sss srsiiji aaaa a s ti
• It	•
Hi—rnfinfti
s
a
X
lltf
T
23.33
4-t
35.00
TiM din)
44.0
58.2
000272

-------
Nelson Analytical 2700 Chromatography System Report Header
sssassaassas
Samp 1e Name :
Samp Ie Number:
Operator	:
Interface # :
AutoSampler :
Rack/Vial '
PCB1221
5	Channel
None attached
0/0
T ime
Study
8/29/89 8!57 AM
MCFARLAND
A/D mV Range » 1000
Data Acquisition Timei 8/29/89
Delay Time	s 0.00 min.
End Time	: 70.00 min.
Sampling Rate : 1.0 pts/sec
8s28 PM
Raw Data File	5
Result File	s
Instrument Files
Process File	:
Sample File	'•
Sequence File	t
Inj. Volume	'•
Sample Amount	:
C:\2700\GC5\MCF5011. raw
Cs\2700\GC5\MCF50i1. rst
C:\2700\GC3\F0E. ins
C:\2700\GC5\EXSTD.pre
CS\2700\GC5\MCC1221.smp
C:\2700\GC5\MCFS4A.seq
2 uL
1.0000
uni ts
Noise Thresholds 1
Dilution Factors 1.00
Divisor	: 1.0000
Area Reject	s 0.00
Area Threshold : 100
Multiplier	s 1.00
Additive Constants 0.00
Bunch Factors i
Instrument Conditions!
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15
PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected!
Ret Time
[min 3
1.62
1.81
5.72
7.	18
8.	13
9.36
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L	C uV-sec 3
*********
Peak Ht
CuV3
Raw Amount
ug\L
389663.69 779327.38 276148.03 389663.69
000273
2408061.00
1509.25
349.00
1827.25
6982.00
4.81e6 175438.78
3018.50
698.00
3654.50
•j33.43
80. 73
er*T
748.20
*408061.00
1509.25
349.00
1827.25
6982.00

-------
I
To
I
9.94

10.31
PCB1221
12.87

13.28

14.59

16.92

17.81

18.55

19.92

20.37

21.31

27.55

o0.53

35.37

38.82

42.47

44.32

46.49

47.69

49. 17

52.69

57. 17

60. 19

61.34
DBC

A>'V, *
So
/v y iD'
c -V4
4024.13
0.00
437.28
2896.33
228.30
1982.49
722.73
374.50
4231.67
6666.38
1249.18
305.00
243.50
195.00
336.25
309.00
142.00
376.00
2378.00
233.50
180.25
355.75
1515.00
0.00
874.56
5792.66
437.00
3964.98
1443.50
749.00
2498/33
610.00
487.00
390.00
672.50
618.00
284.00
732.00
4736.00
307.00
360.49
711.50
3030.00
69733.00
602.69
1870.65
90.72
266.02
57. 13
203.81
105.43
61.27
240.14
323.26
148.46
46.59
44.91
36.90
66.44
66.95
25.62
67.77
176.30
48.01
32. 93
65.55
296.14
6456.44
4024.13
0.00
437.28
2896.33
228.50
1982.49
722.73
374.50
4251.67
6666.58
1249.18
305.00
243.50
193.00
336.23
309.00
142.00
376.00
2378.00
253.50
180.25
355.75
1515.00
0.00
tal Area = 5786695.00
Total Concentration = 2837815.0000
^port by Doherty Bresnahan
000274

-------
FileNaaa : C: \2700\GC3\MCF3011-ra*	Data: 8/29/89 8:SB AH Paga 1 of 1
Start Tiaei 0.00 ain End Tiaet 70.00 ain Low Points 5113 uV High Point: 275859 uV
Vertical Scala Factort 0.00 Plot Q«s«t: 0 aV Plot Seals: 100 aV
Chroaatogra*
9 99
mm-.
m
S
a
n
«
11.(7	23.33	35.00	58.33
Tit* (ain)
000275

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
flnple Number
'P srator
I
ter-face #
toSampler
ck/Vial
PCB1232
5	Channel
None attached
0/0
Time
Study
8/29/89 9«17 AM
MCFARLAND
A/D mV Range : 1000
Ita Acquisition
lay Time
End Time
Imp ling Rate
m Data File
Result File
instrument File
¦ acess File
™mple File
Sequence File
| j. Volume
Sample Amount
Iise Threshold
lution Factor
Divisor
Timet 8/28/89 9«42 PM
0.00 min.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5012.r aw
C:\2700\GC3\MCF3012A.rst
C:\2700\GC3\F0E.ins
CJ\2700\GC5\EXSTD.pre
C:\2700\GC5\MCC1232.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
J 0.00
00
0000
Area Threshold
Multiplier
Additive Constant
100
1.00
0.00
Bunch Factor
I
I
I
I
V
strument Conditions:
pillary SC -
Instrument	:VARIAN
Column	:	.2SMM
Column Length	:	30M
Carrier Gas	s	HE
Flow Rate	:	20CM/SEC
Split Ratio	:
Temperature	:	160
Injection Temp.:	200
Detector 1	:	300
Detector 2	:
Notes	:
3400
ID .25UMFILM
RTX3
LINEAR VELOCITY 15 F'SI
1/MIN TO 230
tal Number of Peaks Detected* 46
Ret Time
^min]
1.62
1.80
5.69
7. 16
8.09
9.32
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L	CuV-sec3
*********
Peak Ht
CuV3
Raw Amount
ug\L
215568.05 431136.09 183862.00 215568.05
000276
1302256.73
846.50
248.00
848.00
3452.37
2.60e6
1693.00
496.00
1696.OO
6904.73
96131.67
182.12
50.69
128.68
389.91
1302256.75
846.50
248.00
848.00
3452.37

-------
9.90
10.26
11. 54
13.21
13.87
14.53
16. 03
16.22
16.85
17.76
18.46
19.75
20.24
20.66
21.02
22.41
22.73
23.75
24.67
26. 03
26.49
26.98
27.39
29.	43
30.	10
30.48
31.	14
s-» • /
•jo .98
34.53
-^•5. wO
36.82
39.05
42. 47
42.81
46. 50
57. 20
60.21
61. 37
PCB1232
^ , 0'
DBC
2179.42
13455.66
163.25
0.00
434.50
6789.00
887.93
1509.50
20181.50
7583.50
4174.00
160.00
3041.96
3203.67
4245.91
4510.39
4733.86
6932.00
1498.00
237.98
2800.63
5133.37
6662.-37
377.25
6343.71
572.25
1133.81
606.18
571.00
1029.00
614.75
1664.51
348.50
1106.30
297.40
914.64
344.00
459.00
1363.75
0. 00
4358
jj.q% 50
'. uo
13578.00
1775.85
3012^00
8348.00
320.00
6083.92
6407.34
8491.81
9020.77
9467.72
; / .<•	f
2996.00
475.96
5601.27
10266.73
13324.73
754.50
12687.42
1144.50
2267.63
1212.36
1142.00
2058.00
1229.50
3329.02
697.00
2213.00
594.81
1829.23
688.00
913.00
2727.50
63736.00
341.98
1327.12
39.56
914.88
70. 14
757.04
181.64
196.00
2037.57
867.89
612.13
36.21
422.93
430.83
387.38
676.62
568.35
800.63.
194.02
37.57
401.17
739.07
801.09
41.50
863.77
82.60
159.43
95.38
86.95
163.12
94.77
253.53
68.54
152.94
53.95
141.80
55.95
37. 33
260.43
5912.12
2179.42
13455.66
163.23
0.00
434.50
6789.00
887.93
1509.50
20181.50
7583.50
4174.00
160.00
3041.96
3203.67
4245.91
4510.39
4733.86
6932.00
1498.00
237.98
2800.63
5133.37
a662.37
¦377. 25
6343.71
572•25
1133.31
606. 18
571.00
1029.00
614.75
1664.51
348.50
1106.50
297.40
914.64
344.00
459.00
1363.75
0. 00
Total Area = 3369002.25
Total Concentration = 1641484.1250
Report by Doherty Bresnahan
000277

-------
r Maaa 1 C:\2700\8C3\)CF3012.rai»	Data' 8/29/89 9s 18 AH Pap 1 of 1
tart Ti«t» 0.00 ain End Tiaf 70.00 ain Loh Pointt S104 uV High Point: 189075 uV
Meal Scali Factors 0.00 Plot Qffwts 0 aV Plot Scalts 100 aV
Chrotatograa
Ml
I
I J* tus53??3;s 3S	3 s e it
11M
23.33
3101
TIm (ain)

54,33
000278

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
PCB1242
laaaaaaasaaaasaaaa
Time	: 8/29/89 9:20 AM
Study	: MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range '• 1000
Data Acquisition Time: 8/28/89 10:57 PM
Delay Time
En d T i me
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
0.00
70.00
1.0
min.
min.
pts/sec
Ci \2700\GC5\MCF5013. raw
C:\2700\GC5\MCF5013.rst
C:\2700\GC5\F0E.ins
C:\2700\6C5\EXSTD.pre
C:\2700\GC5\MCC1242.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 units
Area Reject
: 0.00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold s 100
Mu11 i p1i er	: 1. 00
Additive Constant: 0.00
Bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PSI
160
200
300
1/MIN TD 230
Total Number o-f Peaks Detected: 54
Ret Time
Cmin D
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
ug\L	CuV-sec3
*********
Peak Ht
CuV]
Raw Amount
ug\L
1.62
1.81
8.07
9.32
9.90
10.25
103842.61 207685.22
745721.69 1.49e6
0002*79
459.25
1388.38
1424.64
10698.52
918.50
2776.75
2849.27
21397.03
92757.36
51465.13
81.62
162.44
216.59
1068.89
103842.61
745721.69
459.25
1388.33
1424.64
10698.52

-------
11.34
i^« 20
13.87 PGB12#"2-&^>
14.52
16.02
16.20
16.84
17.74 -P06 lO-fa-
lS. 43
18.92
19.73
20.23
20.64
21.00
22.38
22.71
23.72
24.64
23.33
26.00
26.46
26.94
27.36
28.33
29.43
30.07
0 • 43
31.09
32.32
"?T
¦ dm 4^
33. 93
34.46
33.27
36.77
-»'9 .
38.99
42.43
42.76
44.26
46.47
49. 14
49.90
32.69
33.49
57. 19
60.21
61.37


Q&O
63.24 -©66—Q&
797.99
19043.67
0.00
12821.30
1703.86
3131.30
37962.33
13464.88
10810.38
2830.80
714.98
6233.36
6511.12
8067.00
8887.04
9172.16
13979.67
2939.11
371.00
565.06
5928.30
10269.92
13598.84
1160.70
12727.04
1223.36
2341.19
1302.26
193.50
1270.44
2367.13
1241.00
3661.00
786.30
146.00
2389.50
372.10
2181.83
295.00
659.00
637.50
217.00
421.00
196.50
998.00
1463.30
32498.00
0.00
1395.98
2234.00
25643.00
3407.73
6263. Oi"
21620.77
5701.59
1429.95
12470.72
13022.24
16134.00
17774.08
18344.31
s8/o.
742.01
1130.13
11836.59
20339.84
25454.08
2450.73
4682.38
2604.32
386.99
2340.88
4734.23
2482.00
7322.00
1373.00
292.01
5179.00
1144.20
4363.70
590.00
1318.00
1275.00
434.00
842.00
393.00
1996.00
2927.00
64996.00
747.00
109.42
797.99
1377.39
19043.67
166.39
0.00
1447.99
12821.50
370.11
1703.86
381.34
3131.50
3786.24
37962.33
1692.06
13464.88
1309.32
10810.38
329.97
2830.80
104.77
714.98
872.94
6235.36
897,94
6311.12
799.62
8067.00
1314.06
3887.04
1093.44
9172.16
1610.70
13979.67
397.91
2939.11
68.67
371.00
90.04
563.06
844.68
5928.30
1488.07
10269.92"
1606.41
13598.84
111.28
1160.70
1742.34
12727.04
180.06
1223.36
323.48
2341.19
204.18
1302.26
36.24
193.50
189.07
1270.44
356.44
2367.13
206.41
1241.00
559.86
3661.00
139.88
786.50
30.74
146.00
365.16
2589.50
102.29
572.10
339.68
2181.35
40.32
293.00
105.99
659.00
110.88
637.50
45. 12
217.00
77.77
421.00
34.92
196.50
174.90
998.00
273.46
1463.50
5968.11
32498.00
63.84
0.00
3tal Area » 2236006.75
lotal Concentration = 1126312.8750
Report by Doherty Sraanahan
000280

-------
FileNaaa : C:\2700\H3\MCF5013.rM	Data: 8/29/89 9:21 AH Page 1 of 1
Start Tiati 0.00 tin End Ti«a» 70.00 ain Lou Points S124 uV High Point: 96014 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 aV Plot Scale: too aV
Chiciatograi
1MH
ns>A
an ftgsos.sis assusfc asRts ;:t t t 7, *
««« s SSSCSI RGKKEJI »HB*« ? 5 S T B 6 8 8
S
i ^
a
«i
ft
3J3-:
MKhz
m
Trrinttnfffimwniiiriifiiiiiiiiiiii 11—711111 mi iiii 11 ml
111"
<117
11.(7
23.33
35.01
Tim* (nn)
3.33
000281

-------
Nelson Analytical 2700 Chromatography System Report Header
>amp le Name
sample Number
Operator
PCS1248
Time
Study
8/31/8? 10!SO AM
MCFARLAND
Inter-face # : 5
AutaSampler : None
Rack/Vial : O/O
Channel
attached
A/D mV Range s 1000
Data Acquisition
De1ay T i me	s
End Time	s
Sampling Rate :
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Times
0.00
70.00
1.0
8/29/89
min.
min.
pts/sec
11 AM
C•\2700\GC5\MCF3014.raw
C *\270O\GC5\MCF5014A.r st
C!\2700\eC5\F0E.ins
C:\2700\6C5\EXSTD.prc
C:\2700\SC5\MCC124a.smo
C:\2700\8C5\MCF54A.seq
In,j. v'olume
Sample Amount
2 uL
1.0000 units
Area Re.iact
0. 00
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Area Threshold : 100
Multiplier	: i.00
Additive Constants 0.00
E'unch FjctOf'!
Instrument Condi t ionst
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sol it Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PS!
160
200
300
1/MIN TO 230
Total Number of Peaks Detected* 58
F:et Time
C m i n 3
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
'.tq\L	CuV-secJ
*********
Peak Ht
C uV ]
Raw Amount
uq\L
1
1
10
U
62
32
26
51
13. 17
14.53
000282
143038.72 286077.44 116677.09 143038.72
'82969.63
258.00
181.75
8837.75
6059.51
1.56e6
516.00
363.50
17675.50
12119.02
>743. 28
47.08
27.68
719.64
654.60
•32969.63
253.00
181.75
8837.75
6059.51

-------
16. 03
16.85
17.78
18. 46
18.95
19.74
20. 23
20.65
21.00
22.	40
"7
23.73
24.64
25.34
26.02
26. 46
26. 94
27.36 Otb |24£
23.	25
29.	43
30.	08
30.	44
3 i. 09
31.'73
(y* < y
\0s

¦
255.00
31974.16
9370.27
6657.25
3514.02
849.47
10787.00
10040.14
13589.87
14705.70
10920.51
22701.16
4304.86
274.50
929.66
12329.74
19152.49
27638.13
1857.81
23414.69
2798.48
5757.91
4099.74
144.00
510.00
18740.55
13314.50
7028.05
• 1698.94
21574.00
20080.23
27179.73
29411.41
21841.
3509. 72
549.00
1859.31
24659.43
61.34
61.71
. 21
O-J
64.06
68. 70
"4011. 75
1466.50
0.00
688.25
306.50
11515.31
3199.48
-ob • C
3*.. "-<2
39^.75
7=4.50

3165.21
6--,*j,0. 4 c*
33. 92
3831.67
11663.34
34.45
3801.75
7603.50
35. 27
36.75-FCB124b Grf
9813.00
19626.00
0. 00
57 46•00
33.29
553.92
1107.84
33.97
8089.50
16179.00
40. 49
551.50
1103.00
41 . 53
228.75
457.50
42. 40
1488.85
2977.70
42. 75
"738 1. 09
14762.19
44. 22
609.25
1213.50
4o .43
2384.99
4769.95
46. 73
271.00
542.00
49. 1 1
6o7.00
1334.00
49.87
360.00
720.00
50.50
40 1.00
802.00
cr i, cr
J— • O-J
634.50
1269.00
53. 47
373.25
7 46.50
56. 13
144.75
289.50
57. 15
2627.00
5254.00
60. 17
1469.50
2939.00
•.> • 0 0
924.00
1376.50
613.01
60. 88
255•00
3082.99
31974. 16
905.05
9370.27
774.31
6657.25
368.51
3514.02
123.24
849.47
1439.13
10787.00
1388.01
10040.14
1ww9.86
13589.87
2073.64
14705.70
1346.52
10920.51
2535.57
22701. 16
561.25
4304.86
50.63
274.50
138.57
929.66
1686.27
12329.74
2664.52
19152.49
3174.67
27638.13
225.79
1857.31
31 14.80
23414.69
409.23
279Q.48
737.33
e- ^ ir -r o i
•J / w / . 7 I
;*:e; .
40-39. 7 4
i ¦ 'Jo
1 , vlj
74.9©
397.25
467.34
' C" 4
i O J • *
975.72
5831.67
614.14
3801.75
1468.26
9813.00
416.73
0. 00
92.09
55-i. 92
1169.29
3089.50
98. 92
551.50
39.30
~ Iff
^_«.o • / u
250.65
1488.35
1139.48
¦'381.0?
3. 56
c>09, 25
35t.31
2394,99

271.00
119.49
667.00
70. 02
360.00
73. 90
401.00
111.31
634.50
66. 49
Iff
/ -J • _
28. 60
144.75
467.35
2627.00
283.24
146V.50
6238.42
34011.75
236.07
1466.50
84. 77
0. 00
95. 04
688.25
56. 94
306.50
Total Area = 2540929.25
Total Concentration = 1267129.6250

-------
FileNa* : C:\2700\S3\ICROU.riii	0»t«: 8/31/89 10:31 AH Pa
-------
Samp 1e Name
Sample Number
Operator
Interface #
AutoSampler
Rack/Vial
PCB12S4
S	Channel
None attached
0/0
i line
Studv
8/31/8? 10:'
MCFARLAND
AM
A/D mV Ranqe
1000
Data Acquisition Times 8/29/89
De 1 ay Time	: 0.00 mm.
End Time	: 70.00 min.
Sampling Rata : 1.0 pts/sec
1s 25 AH
Raw Data File :
Result File 5
Instrument File:
Process File :
Sample File :
Sequence File :
C:\2700\GC3\MCF5015.raw
C:\2700\GC3\MCF5015L.rst
C:\2700\SC5\F0E.ins
Cs\2700\GCS\EXSTD.pre
C:\2700\GC5\MCC1234.smp
C *\2700\GC5\MCF3 4A.ssq
!nj. Volume
¦ample -¦•.-sount
2 uL
1.0000 units
urea He.isc:'
Noise Thresholds 1
Dilution Factor: 1.00
D i v i sor	s 1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
1.00
0.00
:ur
:n Facsor:
3400
ID .2:
Instrument Conditions!
Capillary GC -
Instrument	:VARIAN
Column	s	.25MM
Column Length	*.	30M
Carrier Gas	:	HE
Flow Rats	:	20CM/1
•Split Ratio	:
Temperature	:	160 1/MIN TO
In j ec 11on Temp.s	200
Detector 1	s 300
Detector 2	:
Notes	i
iUMFILM RTX5
;EC LINEAR VELCCI"
:~o
15 PS I
Total Number of Peaks Detected!
Ret Time
C m i n 3

**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount- Peak Area
u=t\L	CuV-sec 3
*********
Peak Ht
C u V 3
Raw Amount
uq \ L
1.62
1.81
20. 66
21.28
22. 43
00028*:
0.00 37461.45
0.00 438305.53
0.00 18853.78
0.00 7737.98
0.00 2341.20
0.00 12523.00
24992.20
15819.95
1225.10
335.21
138.98
758.23
0. 00
0. 00
0. 00
0. 00
0.00
0. 00

-------
23.77
24.73
26.50
26. 99
27.51
28.28
29.	47
29.76
3Q. 11
30.	48
31.	12
31.94
trey
33. 25
33.95
48
, 84
30
78
, 06
,69
30 I°e<3»
I
40.
40.
41.
4
-------
FileNaae : C:\2700\Ga\MCR015.raw	Date: 8/31/89 10:54 AH Paqa 1 of 1
Start Timet 0.00 ain End Timet 70.00 nin Low Point: 5083 uV Hiah Point: 30048 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mV Plot Scale: 100 aV
ChroMtograi
I
1MM •
R 9t XV	53 S %
 sin u i
_ a
o.tn-9
I
u
n
%
iwrf
C7-1 1
" 3 |\
liiirirrTif^J^TTft^nifiiTifTriiiitrsjri i;i r;n :i!" t
• i' ¦
1U7
B
JL
i
9.S
23.33	35.00
Tiu (»in)

000287

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
EVALB
T ime
Study
8/29/89 i 0:17 AM
MCFARLAND
Inter-face #
AutoSampler
Rack/V/ial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Times 8/29/89 Q:5t AM
Delay Time	: 0.00 min.
End Time	! 70.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File
Result File
Instrument File
Process File
Samp 1e File
Sequence File
C:\2700\GC5\MCF5015F.raw
C:\2700\GC5\MCF5015H.rst
CJ\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C'\2700\GC5\MCCEVAL.=mp
CJ\2700\6C5\MCF54A.ssa
In.j. Volume
Sample Amount
2 uL
1.0000

-------
. 6.66
ENDRIN
0.00
56031.00
4533.08
0.00
40.57

214.50
429.00
33.47
214.50
41.07
000
0.00
1392.00
115.69
0.00
46. 01
DDT
0.00
63538.00
5361.11
0. 00
51.26
ENDKET0
0.00
3907.00
331.97
0.00
60. 22

1818.7S
3637¦50
349.51
1813.75
61. 38
DBC
0.00
53339.00
4892.36
0.00
Total Area = 415266.63
Total Concentration » 19331.3086
:sssass8
Report by Doherty Sresnahan
Q00280

-------
FiliNut < C:\2700\GC3\fCF501T.rw	Oatfi 8/29/89 10S17AN Pap 1 o< 1
Start TiM> 0.00 ain End Tiaai 70.00 ain lot Point: 9028 uV High Point: 16744 uV
Vertical Scala Factors 0.00 Plot Offsat: 0 aV Plot Scala: 100 aV
Chromatogram
%
§
#1
U
11.(7	&S	35.01
, Tia# (aia)
000290

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
100/200 A
Time
Study
8/29/39 5:32 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
s
None
0/0
Channel
attached
A/D mV Range : 1000
Data Acquisition Time» B/29/99 4:17 PM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process rile
Same 1e File
Sequence File
In.i. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
68.97
1.0
min.
min.
pts/sec
C:\2700\GC5\MCF3027a. raw
C:\2700\GC5\MCF5027B.rst
C:\2700\GC5\FOE.ins
C:\2700\GC5\EXSTD. pre
C: \2700\GC5\MCF51A. smp
C:\2700\GC5\MCF54A. sea
2 uL
1.0000 UG/kg
1
1.00
1.0000
Are;. Re.iset	: 0. «X>
Area Threshold : 100
Mu11 i p1i er	; 1.00
Additive Constant: 0.00
Bunch Factor
Instrument Conditions
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
"low Sate
zo1i t Rat l o
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 P5I
160 1/MIN TO 230
200
300
Total Number o-f Peaks Detected: 32
********** EXTERNAL STANDARD REPORT *********
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin]	Name	ug\L	CuV-secJ CuV]	ug\L
12.37
3-BHC

33.09
355367.50
18737.06
93.09
13. 15
HPTCHLR

108.34
210396.00
11356.03
108.24
21.43
ALDRIN

35.34
368311.00
22524.74
35.34
26.05
HEPEF0X

94.57
265676.97
17471.43
94. 57
30. 39
END01
000291
93.74
247216.50
17366.3 7
93. 74
33.33
DIELDRIN
255.80
363847.16
26642.34
255.80

-------
167.36
234.19
137.87
1066.73
233.01
ttal Area = 3254795.00
tal Concentration = 2571.0537
J port by Doherty Bresnahan
38.12 END02	167.36	393028.00	23909.16
41.00 ENDALD	234.19	220685.34	16772.72
45.98 DDT	-1-37.37 216690.22	19038.90
55.92 METHOXY	1066.73 394182.00	36343.93
61.32 DBC	238.01	228886.50	21127.40
000292

-------
FileMiia : C:\2700\GC3\HCF5027a.ra*	Date: 8/29/89 5:33 PH Pagt 1 of 1
Start Ti«: 0.00 ain End Tina* 68.97 sin Lot Point: 5214 uV High Point: 41647 uV
Vertical Scale Factor: 0.00 Plat Offset: 0 nV Plot Scale: 100 aV
Chroiatogra*
S Rft
o rs*i
s 9 t>£ s?s	?
9 s II KS B HO 3
?3S
S| -9 SI
Mill
u
11
5
0.18-
3.S-3
lltt-3 "
¦frfV-
rfr-f'-rifVir
nrrrr
i-r«f f
i
Jt-
* 3
¦ »
3 2
1 S
r. .*11
1L«	22.3!	*.«	45.»	57.47
Til* (ila)
4
000293

-------
I ample Name
ample Number
Operator
Nelson Analytical 2700 Chromatography System Report Header
i
[
iter-face #
nutoSampler
ack/Vial
EVALB
5	Channel
None attached
0/0
Time
Studv
8/30/89 3:05 AM
MCFARLAND
A/D mV Range
1000
ata Acquisition Times 8/30/89 12:54 AM
Delay Time
rnd Time
amp ling Rate
Raw Data File
Result File
I Tstrument File
•ocsss File
Sample File
J"eQuence File
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5033.raw
C:\2700\GC5\MCF5033.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCCEVAL.smp
C:\2700\GC5\MCF54A.seq
f
n j . Volume
Sample Amount
f
oise Threshold
Dilution Factor
i v i sor
2 uL
1. 0000
\
1.00
1.0000
Area Re.iect
Area Threshold
Multiplier
Additive Constant
'JO
100
1 . 00
0. 00
Bunch Factor: 1
nstrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
I
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
2CCM/SEC LINEAR VELOCITY
(¦ ; 3w ta-
5»lit Ratio
Tempera bura
Injection Temp.
Detector 1
Detector 2
Notes
otal Number o-f Peaks Detected: 13
¦>3 I
160 1/MIN TO 230
200
300
f:et Time
C m i n ]
Component
Name
EXTERNAL STANDARD REPORT

Adjusted Amount Peak Area Peak Ht Raw Amount
uq\L	CuV-sec] C uV ]	uq\L
1 . 60
1. 84
>1.47 ALDRIN
24.58
r-4.51 DDE
*•6.65 ENDRIN
G00294
1215.90
13248.3?
0. 00
685.00
0. 00
0.00
2431.79
26496.73
183396.00
1370.00
917.50
79735.50
1494.77
933.74
12354.55
101.19
59.81
6307.80
1215.90
13243.39
0. GO
635.00
0. 00
0. 00

-------
40.50	2366.57	4733.14	296.36
41.07 DDD	0.00	15BS.B6	111.51
45.98 DDT	0.00	50654.00	4530.83
50.56	5002.13	11764.25	103.52
51.23 ENDKETO	0.00	7004.73	442.39
60.20	2656.75	5313.50	499.52
61.37 DBC	0.00	69368.00	6395.22
Total Area = 444771.(56
Total Concentration = 26054.7305
Report by Doherty Bresnahan
2366.57
0. 00
0. 00
5332.13
0.00
2656.75
0.00
00G295

-------
FileNaM : C:\2700\GCS\nCF3033.riw	Data: 8/30/89 8:03 AH Paga 1 of 1
Start Timet 0.00 ain End Tiui 70.00 sin Lom Point: 5213 uV Hiah Point: 17568 uV
Vertical Scale Factor: O.OO Plot Offset: 0 aV Plot Scale: 100 mV
Chrotatogra*
UUHH
«. *
r S 8
M S
St
3S
am-
bjjH
'AM-
11.67	23.33	35.00	48.67	58.33
Ti*e (Bin)
0002OH

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number-
Op era tor
Inter-face #
AutoSampler
Rack/Vial
100/200 B
5	Channel
None attached
0/0
T ime
Studv
3/31/89 12:33 AM
riCFARLAND
A/D mV Range
1000
Data Acquisition
Delay Time
End Time
Samp 1ing Rate
Raw Data File
Result File
Instrument File
Process File
Samp 1e File
Sequence File
T ime:
0. 00
63 « '-'0
1.0
8/30/89
min.
min.
p t s/sec
11:52 PM
C:\2700\GC5\MCF5039i. raw
C:\2700\GC5\MCF5039i. rst
C:Y2700\GC3\F0E.ins
C:\2700\GC5\EXSTD. pre
C:\2700\GC5\MCF51B. smo
C: 2700\GC5\MCF34A.
I n ..i. 7 a 1 ume
S amc 1 e Amou.n t
2 uL
1.0000 UG/kq

Noise Threshold
Dilution Factor
Divisor
1
1. 00
1.0000
Area Threshold
Multip1ler
Additive Constan'
100
1. 00
0. 00
•Bunch Factor-
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flew Kate
ScIit Ratio
T ~mo er a t ur e
I n ,i ac t i on Temp
Detector 1
Detector 2
Notes
3400
ID . 25UMFILM
VARIAN
. 25MM
301*1
HE
20CM/SEC LINEAR
- CI- - L,
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 33
Ret Time
Cmin ]
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
uqv>L	CuV-sec]
Peak Ht
C u'v ]
Raw Amount
u.q\L
10.23 A-BHC
11.90 B-BHC
14.06 D-BHC
21.39 ALDRIN
28.85 G-CHLDANE
30.80 A-CHLDANE
000297
93.46	441920.00
96.01	150262.00
100.79	350087.69
96.37	390024.50
97.53	328867.00
93.43 323979.34
26227.36
S845.55
22337.30
26663.67
24368.64
24459.90
=>5. 46
96. 0 1
100.7°
96. 37
97.55
95. 43

-------
34.38 DDE	190.66 566213.00	46770.93 190.66
136.52 ENDRIN	324.39 283805.00	22039.67 324.39
40.29 DDD	276.33 292701.63	23646.67 276.33
44.41 ENDOSULFATE	195.97 356473.50	27852.94 195.97
51.04 ENDKETO	306.87 317000.00	25482.56 306.87
¦ 61. 18 DBC	334.78 253417.00	22417.21 534.78
™al Area = 4054750.50
otal Concentration = 2210.6040
i_ 	
^ort by Doherty Bresnahan
000298

-------
FilsNi* : C:\2700\GC5\HCF5039i.ran	Dat» 8/31/89 12:59 AH Paqe 1 of I
Start Tio#i 0.00 ain End Tiaes 63.30 ain Lqm Point' +958 uV High Point: 51476 uV
Vertical Scale Factor! 0.00 Plot Offset: i) aV Plot Scale: 100 aV
ChroMcogra*
UWH
a s » 3 a s i! t* ssi & a a s s c	t
** !: si; s is » tuti : : :• s
a w
6 za
tt»-2

•xmr-.
**.*+* m
3
a
•c;o-5
(•a*-3
3-4*-
i I
•' i i1
iV { h
2 i
I I
•M II 1 I
J) it il 11 '
II II I • I I I I I
17r^iliii ii ii iiii Mill tiil i l*TP?'
ii «i i I n iiii
[ i
i i
n i
4*-*-
U
3 S
JU.
10.S
ZLia
31.65
Ti«e (sia)
42.20
52.75
000239

-------
Nelson Analytical 2700 Chromatography System Report Header
Simple Name
.Ample Number
perator
Interlace #
JutoSampler
Rack/Vial
100/200 A
5	Channel
None attached
0/0
Time
Studv
8/31/39 12:13 PM
MCFARLAND
A/D mV Range : 1000
I
ata Acquisition Time! 8/31/89 1:06 AM
elay Time
End Time
amplinq Rate
«
aw Data File
°3suIt File
Instrument File
,-ocess File
¦sample File
~=quence File
|r. . Vo 1 Limi?
sample Amount;
Ioise Threshold
ilution Factor
n i visor
Instrument Conditions:
capillary GC -
Instrument
Column
Column Length
Carrier
-low Rate
cp i, 1-3 Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5043.raw
C:\2700\GC3\MCF3043.est
C:\2700\GC3\FGE.ins
C:\2700\GC3\EXSTD.prc
C: \2700\GC3\NCF31A. ship
C:\2700\GC3\MCF34A.sea
2 uL
1.0000 UG/kg
1
1. 00
1.0000
Ar e a Re ,:ect	: 0. 00
Area Threshold '• 100
Mu11 i p 1 i er	: 1.00
Additive Constant: 0.00
Su.nch Factor:
7ARIAN 3400
.25MM ID .25UMFILM PTX5
30M
' HE
20CM/SEC LINEAR VELOCITY 11 P3I
160 1/MIN TO 230
200
300
I
otal Number o-f Peaks Detected: 34
I
et Time
C m i n ]
Componen t
Name
EXTERNAL STANDARD REPORT *********
Adjusted Amount Peak Area Peak Ht
up vL	CuV-sec] CuV3
Paw Amount
uq ¦- L
12.36 G-BHC
13.12 HPTCHLR
21.46 ALDRIN
26.03 HEPEPOX
30.34 END01
33.77 DIELDRIN
000300
91.34	370461.30
113.69	224182.00
90.07	336447.00
101.45	283001.00
99.76 263070.00
276.09 392701.84
19671.99
12705.06
22971.63
19045.39
18249.64
29239.27
91.34
115.69
90. 07
101.43
99. 76
276.09

-------
33.05 END02
40.92 ENDALD
45.38 DDT
35.81 METHOXY
61. 19 DBC
130.19
247.14
159.36
1233.88
271.35
412398.00
232884.38
250466.22
455948.00
260952.00
30870.06
17585.11
21782.11
40637.35
23087.36
180.19
247.14
159.36
1233.88
271.35
Total Area = 3534511
Total Concentration
= 2866.8120
Report by Doherty Bresnahan
Q00301

-------
FileNua : C:\2700\GCS\nCF3043.rw	Date: 8/31/89 12:14 Ftt Page 1 of 1
Start Tims 0.00 sin End Tia«: 70.00 ain Lom Point: 3069 uV High Point: 45642 uV
Vertical Scale Factor: 0.00 Plat Offset: 0 aV Plot Scale: 100 aV
Chiotatograi
1N.I
0.3J-
*«K
aaH
it tn_3 ^
5 ii
5 sa " 83 3 * C.ilSS * 5,a SS6; SfJ.i
355 ; i; sua an** ?	Rtma
T
I a I til
.1. il ii II
M ~	TTilnniTTrr^iri'rraif!
( in > ' (<
iS § I r § i 8 x
a	s 3, s ? ,*, 3 ?
11.W	23.33	3. DO	*.W	58.3
Ti&e ruin)
000302

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
PBLK-1
Lab Name: LOCKHEED-ESC
Contracts 68-03-3249
Lab Codes	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOW
'/. Moisture: not dec. 0 dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
SAS No.:	SDGi No.:
Lab Sample ID:	9S187RB
Lab File ID:		
Date Received:	7-23-89
		Date Extracted:	7-31-89
SONC	Date Analyzed:	"I
Dilution Factor:	10
CONCENTRATION UNITS:
UQ/kq	Q
319-84-6	
319-85-7	
319-86-8	
58-89-9	
76-44-8	
309-00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
33213-65-9	
72-54-8	
1031-07-8	
50-29-3	
72-43-5	
53494-70-5	
5103-71-9	
5103-74-2	
8001-35-2	
12674-11-2	
11104-28-2	
11141-16-5	
53469-21-9	
12672-29-6	
11097-69-1	
t1096-82-5	
-alpha-BHC		160
-beta-BHC		160
-de 1 ta-BHC		160
-gamma-BHC (Linaane)		160
-Heptach lor		160
-A 1 dr in—		160
-Heptach lor epoxide		160
-Endosul -fan I		160
-Dieidrin		320
-4, 4'-DDE		320
-Endrin		320
-Endosul-fan II		320
-4,4' -DDD		320
-Endosul-fan sulfate		320
-4, 4' -DDT		320
-Methoxych lor		1600
-Endrin ketone		320
-alpha-Ch lor da.ne		160
-gamma-Chlordane		160
-To'/aphene		3200
-Aroc lor-1016		1600
-Aroc lor-1221		1600
-Aroc lor-1232		1600
-Aroc lor-1242		1600
-Aroc lor-1248		1600
-Aroc lor-1254		3200
-Aroc lor-1260		3200
U
U
U
U
U
U
U
!J
U
U
U
IJ
U
IJ
u
u
u
u
u
u
U
u
IJ
u
FORM 1 PEST
1/87 Rev.
000303

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : PBLK1
Sample Number: 9S187RB
Operator :
Time
Study
8/30/89 1:27 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
12:48 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR018.raw
e:\pkd\MCFR018.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e: \pkd\clpa. snip
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0. 00
*****EXTERNAL STANDARD REPORT*****
ssssssssssssssssa:ssssas=ssss=ss=ss=sssssssss==sss:s===5=;=ss==ssssss
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Rat Tlaa	Component	Adjusted Amount Raw Amount Peak Area Peak Ht MULTIPLIER
[rain]	Nam	-UCAb—	UG/L (uV-sec} [uV] Ad J/Raw
L.45
25.60 0BC	71.45 216.50 2.88e6 65203.52 0.33
Total Area - 2887785.75
total Concentration ¦ 71.4454
Report by Tim Rand, Lockheed-ESC
Q00304

-------
Chromatoqram
FilcNaae : e:\pkd\HCFR01B.rau	Date: 8/30/69 1:27 PM Page 1 of 1	^
Start Tiw: 0.00 ain End liae: 47.00 sin low Point: -1217S17 uw High Point: 2009310 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 «V Plot Scale: 250 ifiV
CN
2S0.000
200.333
166.667
125.000
41.667-
-0.000
7.83	l'j.67	23.50	31.33	39. 17

-------
Nelson Analytical 2700 Chromatography System Report Header
2:15 PM
Sample Name : PBLK1
Sample Number: 9S187RB
Operator ;
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
12:48 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR018.raw
e:\pkd\MCFR018A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 0.00
* * * * * EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
*at tin*	Coopenant	Adjuittd Amount Raw Amount Peak Acta	Peak Bt MULTIPLIER
[mini	Hum	.—UC/L [uV-»«el tuVJ Adj/Raw
21.14 ESCOffll.FAIE	 -	a tomn "n ¦¦jsi.os 8, a a— VCL
25.SO BBC	85.36 228.68 2.38*6	65203.52 9.33
Total Araa - 2990955.75
lotai Concentration • 39.1*08

Report by Tim Rand, Lockheed-ESC

000306

-------
Vertical Scale factor: 0.00 Plot Offset: 0 mV Plot Scale: 250 mV
•—"	uS
CM	CM CM
CLf
CD
cr>
OL>
250.000.
208.333-
166.667-
125.000-
83.333-
41.667-
-0.000-
I I
Jc.-1
f i i"i f i i i i pT i it i i»t i r | i i i i i i i | i it i i i i i i | i i i
7.83	15.67	23.50	31.33
Time (min)
V H g
.g-P —
63
S
hi
i i i i i | i i i i i i i i i
39. 17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : PBLK-1
Sample Numbers 9S187RB
Operator	:
Time
Study
8/29/89 9:47 AM
MCFARLANDl
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range : 1000
Data Acquisition Time:
Delay Time
End Time
Sampling Rate
8/29/89
0•00 m i n.
70.00 min.
1.0 pts/sec
2:39 AM
Raw Data File :
Result File :
Instrument File:
Process File :
Sample File :
Sequence File s
Inj. Volume :
Sample Amount
Noise Threshold
Dilution Factor
Divisor
C:\2700\GC5\MCF50ISA.raw
C:\2700\GC5\MCF5015A.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C: \2700\GC5\MCF54A. seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Multiplier	: 0.33
Additive Constants 0.00
Bunch Factor: 1
Instrument Conditionss
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Sp 1 i t Rat io
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY
eg I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 11
EXTERNAL STANDARD REPORT
Ret Time	Component	Adjusted Amount Feik Area Peak Ht Raw Amount
Cmin]	Name	.-«iTXtT\,	CuV-sec] CuV]	uq\L
-5-1.51
nLDniN	
	o. i;*8—
—1 07 i 00

	i 26 *
55.79
MCTI10XV	
	2*7'?
2609,50—
—195.16	
		
61.37 DBC	94.77 247029.00 16455.54	256.88
MV
Total Area = 251059.50
000308

-------
Total Concentration = 87.2627
Report by Doherty Bresnahan
0003D1

-------
FileNaw : C:\Z700\6C5\MCF3013A.rw	Data: 8/29/89 9:47 AH Paga 1 of I
"Lvt Tim 0.00 sin End Tiax 70.00 iin low Point: 4893 uV High Point: 88844 uV
I "tical Seals Factor: 0.00 Plot Offset: 0 aV Plot Seals: 100 aV
™	Chmatograa
I
1NJI
ILS}-:
9SSH
asfi
l 5
TOT
*	1	m
*	i| n
*	• -
ft
x
t—rr
>i	it
X
1117
1 | | 1 I j
i i r. i i ?i i 9 [ i it i rii
as
35.00
Til* 
-------
_Nelson Analytical_2700 Chromatography System Report Header
Sample Name : PBLK-1
Sample Number: 9S187RB
Operator	:
Inter-face #
AutoSampler
Rack/Vial
T ime
Studv
8/29/99 1:59
MCFARLA.ND
PM
5	Channel
None attached
0/0
A/D mV Ranqe : 1000
Data Acquisition
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Time: 8/29/89 2:39 AM
0. 00 m in.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MCF5015A.raw
C:\2700\GC5\MCF5015E.rst
C:\2700\GC5\FOE.ins
C:\2700\GC3\EXSTD.prc
C:\2700\GC5\MCF51B.smp
C:\2700\GC5\MCF54B.seq
Ini. Volume
Sample Amount
2 u.L
1.0000 UG/kq
Area Reject
0.
Noise Threshold
Dilution Factor
Divisor
1
1.00
1.0000
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow R.afee
SpI11 Rat io
T emperature
In.iectian Tsmp
Detector 1
Detector 2
Notes
Area Threshold
Mu 11 i p1i er
Additive Constant
100
0. 33
0.00
Bunch Factor
3400
ID .25UMFILM RTX!
VARIAN
. 25MM
30M
HE
20CM/SEC LINEAR
VELOCITY 15 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 11
EXTERNAL STANDARD REPORT
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
Cmin]	Name	CuV-sec] CuV]	u.g\L
14. 34-
D DilC 	
	0. 03	334. 00
	29.03	
	0. l'j	
Jl.-jr
MLUM'tP*
'J • [J r IV /' ^

o"7->
61. 37
DBC
107.69 247029.00
16453.54
326.34
Total Area = 249784.00
000311

-------
| tal Concentration = 107.8505
J[port by Doherty Bresnahan
000.31*:

-------
FileNaa* : C:\2700\GC3\HCF50l5A.raw	Date: 8/29/89 1:59 PM Pag# I of I
Start Tinas 0.00 ain End Tines 70.00 Bin Loh Point: 4893 uV High Point: B6844 uV
Vertical Seals Factor: 0.00 Plot Offset: 0 aV Plat Scale: 100 sV
Chroiatogras
11
II
5
3b
n i
j * i
. u
i S!
a
- ». »
a » s
3
*
*
a
9
£
*
9
II
s
1U7
23.33
35.00
4U7

tt.33
TiM (unj
Q003I3

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHEET
fcPA SAMPLE NO.
F'BLK-2
Lab Name: LOCKHEED-ESC
Contract: 68-03-3249
Lab Cods:	 Case No. :
Matrix! (soil/water) SOIL
Sample wt/vol: 30 grams
Level: (low/med) LOU
'/. Moistures not dec. O dec.
Extraction: (SepF/Cont/Sonc)
GPC Cleanup: (Y/N) Y pH:
CAS NO.
COMPOUND
3AS No. : —	SDG No. :
Lab Sample ID: 9S197RB
Lab File ID* 	
Oata Received! 7-25-99
		Date Extracted: 8-1-89
SONC	Date Analysed:
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	
319-85-7	
319-86-8	
58-89-9	
76-44-8	
309—00—2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9—
72-54-8	
1031—07—8	
72-43-5	
53494-70-5—
5103-71-9	
5103-74-2—
8001-35-2	
12674-11-2-
11104-28-2-
11141-16-5-
53469-21-9-
12672-29-6-
11097-69-1-
11096-82-3-
-a 1 pha-BHC		ISO	U
-beta-BHC		160	U
-de 1 ta-BHC		160	U
-gamma-BHC (.Lindane)		160.	U
-Heptachlor		160	U
-Aldrin		160	U
-Heptachlor epoxide		160	U
-Endosul -fan I		160	U
-Dieldrin		320	U
-4,4' -DDE		320'	U
—Endr in		320	U
—Endosul-fan II		320	U
—4, 4' -DDD		320	U
—Endosul-fan sul+'ate		320	U
— 4,4'-DDT		320	U
—Methoxychlor		1600	U
—Endr in ketone		320	U
—alpha-Chlordane		160	U
—gamma-Ch lor dane		160	U
—Toxaphene		3200	U
—Aroc lor-1016		1600	U
—Aroc lor-1221		1600	U
—Aroc lor -1232		1600	U
—Aroc lor-1242		1600	U
—Aroc lor-1248		1600	U
—Aroc lor-1254		3200	U
—Arocloi—1260		3200	U
FORM 1 PEST
1/87 Rev,
000314

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :	PBLK2 Time	: 8/30/89 1:29 pm
Sample Number:	9S197RB Study	: MCFARLAND
Operator :
Interface # :	2 Channel : B A/D mV Range : 10000
AutoSampler :	Varian 8000 without controller
Rack/Vial :	255/255
Data Acquisition Time: 8/30/89 1:39 AM
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate	: 1.0 pts/sec
Raw Data File	: e:\pkd\MCFR019.raw
Result File	: e:\pkd\MCFR019.rst
Instrument File: e:\pkd\pkd.ins
Process File	: e:\pkd\pextstd.prc
Sample File	: e:\pkd\clpa.smp
Sequence File	: e:\pkd\MCFRLND.seq
Inj. Volume	: 2 uL Area Reject	: 0.00
Sample Amount	: 1.0000 uL
~~~~~EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
•
Ret Tim Coopooant Adjusted Amount Raw Amount P«*k Arcs	Peak Ht MULTIPLIER
[mini Him UC/L [uV-j«cl	[uV] Adj/lUv
ta.t* OHBOliD	1.91	S-rM	¦0000.08	ia8>.18	M)	
25.62 DBC 73.72 223.39 2,97.6	66010.27 0.33
Tool Ar»» - 3019722.73
Total Concentration - 74.7260
Report by Tim Rand, Lockheed-ESC
000315

-------
Chromatogram
filename : e:\pkd\MCFR019.raw	Date: 8/30/89 1:29 PH Page 1 of 1
Start Tine: 0.00 Bin End liae: 47.00 nin Lou Point: -2105297' uV High Point: 101S940 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 OV Plot Scale: 250 mV
c
-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name :	PBLK2 Time	: 8/30/89 2:17 PM
Sample Number:	9S197RB Study	: MCFARLAND
Operator :
Interface # :	2 Channel : B A/D mV Range : 10000
AutoSampler :	Varian 8000 without controller
Rack/Vial :	255/255
Data Acquisition Time: 8/30/89 1:39 AM
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
Raw Data File	:	e:\pkd\MCFR019.raw
Result File	:	e:\pkd\MCFR019A.rst
Instrument File:	e:\pkd\pkd.ins
Process File	:	e:\pkd\pextstd.prc
Sample File	:	e:\pkd\clpb.smp
Sequence File	:	e:\pkd\MCFRLND.seq
Inj. Volume	: 2 uL	Area Reject	: 0.00
Sample Amount	:	1.0000 uL
»EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
Rac Tina	Cooponant	Adjuatad Amount Raw Amount Peak Araa Ptak He MULTIPLIER
[mlnj	Naaa	Uc/L [uV-»ael ;uv|	AdJ/Raw
ei.io DiiDOQWirotD	o.tfl iq.63 io?om «« .piai i.33
23.62 DBC	88.03 256.91 2.97.4 66030.27 0.33
vk.
Total Araa • 31*7572.73
Total Coneanttatien » 9a.2270
Report by Tim Rand, Lockheed-ESC
000317

-------
Chromatogram
Filename : e:\pfcd\HCFR019.rau	Date: 6/30/69 2:17 PH Page 1 of 1
Start liae: 0.00 Bin End liae: 47.00 ain Lou Point: -2105297 uV High Point: 1016940 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 mV Plot Scale: 250 mV
cd
250.000
166.667
Of
125.000
-0.000
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Samp 19 Name :
Sample Number:
Operator	:
Inter-face #
AutoSamp lor
Rack/Vial
PBLK-2
9S197RB
S > Channel
None attached
0/0
Time
Study
8/29/89 9:49 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition Time: 8/29/89 3:54 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noi9e Threshold
Dilution Factor
Divisor
0.00 min.
70.00 min.
1.0 pts/sec
C:\2700\GC3\MCF5015B.raw
C:\2700\GC5\MCF5015B.rst
C:\2700\GC5\F0E.ins
C:\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51A. smp
C:\2700\GC5\MCFS4A. seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	: 0.00
Area Threshold : 100
Mu11 i p1i er	: 0.33
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Co1umn
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp.
Detector 1
Detector 2
Notes
VARIAN
. 2SMM
30M
HE
20CM/SEC
3400
ID .25UMFILM
RTX5
LINEAR VELOCITY 15 RSI
160
200
300
1/MIN TO 230
Total Number o-f Peaks Detected) 11
Ret Time
Cminl
**********
Component
Name
EXTERNAL STANDARD REPORT
Adjusted Amount Peak Area
un Vfc *1^/^ CuV-secl
Peak Ht
CuV:

Raw Amount
ug\L
21.36 ALDHIN
34.59 DICLDniN
37.91 ENDQ2
-<>.04-
0. 15-
501.00
636.00
40 ¦ 20
0.12
r6+-
419Q.40
—04.09
209.53
O. 45
1.03 A
55.03 METH0XY
61.45 DBC
	Sr^4	3069« 00	220.21
177.52 517312.00 33732.22
	0.31 l»
537.93
000319

-------
|'tal Area - 525716.50
otal Concentration = 181.0503
Report by Doherty Bresnahan
000320

-------
FilaNua : C:\2700\GC3\NCF3013B. raw	Date* a/29/89 9 M9 AH Paga 1 of 1
Start Tia«< 0.00 tin End Tiaai 70.00 ain Lou Point* 5065 uV High Point: 80882 uV
Vertical Seals Factor» 0.00 Plot Offset: 0 aV Plot Scalai 100 aV
ChxoutograB
lMH
ttat-j
I
I 5U
s.rH
ii

S 5
X ft
T~rr
1
ILff
23.3}	35.06	4.W
TiM (axa)
m 5
n » s*
¦mmf
if I | I s I i i e ! h
,1* ¦ , * ft. I I I I r ¦ 191 , 1-1 ¦ Hi I I 	T i | i M

000321

-------
Nelson Analytical 2700 Chromatography System Report Header
I imp I e Name
imple Number
Operator
I iter-face #
TjtoSampler
Rack/Vial
F'BLK-2
9S197RB
5	Channel
None attached
0/0
Time
Studv
8/29/89 2:01 PM
MCFARLAND
A/D mV Range
1000
I
\ta Acquisition Time: 8/29/89 3:54 AM
belay Time
End Time
| imp 1ing Rate
Raw Data File
Jjesult File
¦	istrument File
¦	¦acess File
Sample File
iequ.ence File
I
0.00 m i n.
70.00 min.
1.0 pts/sec
C: \2700\GC5\MCF3015B.raw
C:\2700\GC5\MCF5015F.rst
C:\2700\GC5\FQE.ins
C:\2700\GC5\EXSTD.prc
C:\2700\GC5\MCF5IB. smp
C:\2700\GC5\MCF34B.seq
i i. Volume
Sample Amount
fjise Threshola
dilution Factor
1 i v i sor
i
2 uL
1.0000 UG/kg
1
1. 00
1.0000
Area Re.iset
Area Threshold
Mu11 i p1igr
Additive Constant

10<
Junch Factor
0. 00
istrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
"low Rate
Split Ratio
T emperature
I n i ec t i on Temp
Detector I
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM PTX3
30M
HE
20CM/SEC LIHEAR VELOCITY
160 1/MIN TO 230
200
300
I
otal Number ot Peaks Detected: 11
EXTERNAL STANDARD REPORT
I
et Time	Component	Adjusted Amount Peak Area Peak Ht Paw Amount
[min]	Name	Cu.V-ssc] CuV]	ug\L
21. 36 hLDRIN	0. 04¦ SO 1. 00	40.20	0.12 '• '>
34 . 59 DDE		u~6.00	34.00	
371 91 CNDRIN		4100, 40	209.53	*¦» 00 :,i
61.45 DBC	225.52 517312.00 53732.22	683.40
otal Area = 522647.50
000322

-------
Total Concentration = 227.2181
Report by Doherty Bresnahan
000323

-------
FileNue : C:\2700VSCS\f1CF5015B.raw	Data: 8/29/89 2:02 Pfl Pag* 1 of 1
Start Tine: 4.00 nin End Ti«e: 70.00 ain Low Point: 5065 uV High Point: 80882 uV
'Vertical Seals Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 oV
Chroaaiograi
5
ji
ai
01
8 5
ft ft
1 * tf
H fc sa
rr
I 1! Ill'

u -
11 - 5 o
M ^ , ,5
—T—
58.33
11.67	23.33	3.00	tt.W
Tiae (ain)
000324

-------
ID
PESTICIDE ORGAN ICS ANALYSIS DATA SHtET
tF'A SAMPLE
OFOIMS F'REG PC
Lab Name: LOCKHEED-ESC
Contract: 68-03-149
Lab Code:	 Case No. :
Matri::: (soil/water) SOIL
Sample wt/vol: 30 grams
Levels (low/med) LOW
7. Moisture: not dec. 1.9 dec.
E:: trac t ion : 
GrC Cleanup: '.Y'/N) N pH:
CAS rJO.
COMPOUND
SAS No. i	SDG No. :
Lab Sample ID:
Lab File ID: 	
Date Received: 7-25-39
			Date Extracted: 7-31-39
30NC	Date Analv:eds * '"j4--" ^ 1
C11 >j. ticn F ac t or:	l C
CONCEN f'RATION UN ITS:
ug/ki	Q
1^ 1*5 ^
319-34-6	
319-85-7	
319-96-3	
58-89-9	
76-44-8	
309-00—2	
1024-57-3	
959_og_g	
1 .-«j-
72-54-3	
1031-07—9—
30-29-3	
53494-70-5-
5103-71-9—
5103-74-2—
8001-35-2—
12674-11-2-
11104-28-2-
11141-16-5-
53469-21-9-
12672-29-6-
1 1097-69-1-
11096-82-5-
-alpha-BHC			32 U
—beta-BHC		32 U
-del ta-BHC		82 U
-gamma-BHC (Lindane;		32 U
-Heptachlor		32 U
—Aldrin		S2 U
-Heptachlor epoxide		32 L!
—En dosu.lt an I		32 U
—	Dieldrin		163 U
-4, 4'-DDE		163 U
—	Endosu.l -fan II		la3 'J
—4,4'-ODD		163 J
—Endosul-fan sul+ate		163 U
—4, 4'-DDT				163 U
—Metho::ych lor		315 U
—Endrin ketone			163
—alpha-Ch lor dane		82
—gamma-Ch lordane		82
—Toxaphene		1631
—Aroc lor-1016		815
—Aroc lor-1221		315
—Aroc 1 or-1232		315
—Aroc lor-1242	:		315
—Aroc lor -1243		315
—Araclor-1234		1631
—Aroc lor-1260		1631
U
u
u
IJ
'J
u
u
u
u
IJ
IJ
FORM 1 PEST
« / r-i t	.
k f O / i» 0 v



-------
Nelson Analytical 27 00 Chromatography System Report Header
1:31 PM
Sample Name : OFOIMS Pre-GPC
Sample Number: 9S185MS
Operator	:
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
2:30 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File	:
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 2 0.raw
e:\pkd\MCFR0 2 0.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
>EXTERNAL STANDARD REPORT*****
Instrument ID:
Varian
3400-1
GC Column
ID: 2250/2401
¦ 	






Ret Tlma
Component
Adjusted Amount Raw Amount
Peak Area
Peak He
MULTIPLIER
[min)
Hum
UC/L
tuV-see]
[uVl
AdJ/Raw







3. J1
G-BHC

46.46 6&.33
1.60*6
177940.98
3.68
4.32
HPTCHLR

50.86 74.80
1.62*6
143254.70
0.68
5.20
ALDRIN

48.64 71.53
1.65*6
124347.70
0.68
11.22
DIEU3RIN

218.93 321.96
6.96*6
184391.83
°-68 \l/






0.68
17.62
DOT
ill <»** 384.04
3.29*6
93006.38
0.68
23.73
DBC

146.ii 213.68
2.87e6
62938.97
0.68
Total Ar«» • 18108400.00
Total Concentration ¦ 773.4702
Report by Tim Rand, Lockheed-ESC
000328

-------
Chromatogram
FileNane : e:\pfcd\MCFR020.raw	Date: 8/30/89 1:31 PN Page 1 of 1
Start Tiae: 0.00 ain End Km: 47.00 Bin Low Point: 5250 uV High Point: 345090 uV
Vertical Scale factor: 0.00 Plot Offset: 0 wM Plot Scale: 250 mV
250.000	
208.333
rrr.^r-f
-0.000	
7.83	15.67	23.50	31.33	39.17

-------
Nelson Analytical 2700 Chromatography system Report Header
Sample Name : OF01MS Pre-GPC
Sample Number: 9S185MS
Operator :
Time
Study
8/30/89 2:19 PM
MCFARLAND
Interface #
AutoSampler
Rack/Vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate ; 1.0 pts/sec
2:30 AM
Raw Data File ;
Result File :
Instrument File:
Process File :
Sample File :
Sequence File :
Inj. Volume ;
Sample Amount ;
e:\pkd\MCFR020.raw
e:\pkd\MCFR020A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
; 0.00
*EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
Rat Tin
[mini
CaopoMusc
Hum
Adjusted Aoouist Saw Amount F**k Arc* P**k He MUIKPLIER
- /js. UC/L (u¥-i«el [uV] AdJ/IUw
5.20 ALPRIH
I, B
11.22 ODE
13.21 EH0KXH
,,,31 7n nwrniat-
23.73 BBC
45.24
	»¦!*»•
66.51
1.6S«6 12414J.J0
237.21
142.52
t.M
148.87
209.51
6.96*6 184191 II
2.91*6 104219.39
1.83 moe.aa—	
HiW-
	*16833.Si	II
173.23
257.69
2.87*6 6293S.97
3.68
} 68
3,68
-r-w-
».»»
3 .si
%-
Total Aim « 13023474.00
Total Concentration - 619.1240
Report by Tim Rand, Lockheed-ESC
000328

-------
Date: 8/30/89 2:19 PH Page
FileNane : e:Vpkd\HCFK020.rau			-		 . .
Start Tiae: 0.00 aio End Tfae: 47.00 ain Lom Point: 5250 uV High Point: 345090 uV
Vertical Scale factor: 0.00 Plot Offset: 0 M Plot Scale: 250 mV
Chromatogram
1 of i	^

cr
<=>
eox.
CO
a->
CXL
250.000-
208.333-
166.667-
125.000-
83.333-
41.667-
c
o
o
CJ
pj-ooo-
CD
-	i rs i^s	C>* C*s«	«qr
Cn S ts S	ovj u-i
r-J u>' od zz Z2 td

V
II
M
o	—in
•— -*r in
cn	rs CN

. r'n	f ;"n
i r^i f3! i i i i^f i i*t
7 .83
15. 67
23 . 50
31.33
39.17

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number:
Operator	:
Inter-face #
AutoSampler
Rack/Vial
MS pre-gpc
9S185MS
5	Channel
None attached
0/0
T ime
Study
8/29/89 9:32 AM
MCFARLAND
A/D mV Range : 1000
Data Acquisition Times 8/29/89 5s08 AM
Delay Time
End Time
Sampling Rate
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
Inj. Volume
Sample Amount
Noise Threshold
Dilution Factor
Divisor
0.00
70.00
1.0
mxn.
min.
pts/sec
C:\2700\GC5\MCF5015C.raw
C:\2700\GC3\MCF5015C.rst
C:\2700\GC5\F0E.ins
Cs\2700\GCS\EXSTD.pre
C:\2700\GC5\MCF51A.smp
C:\2700\GC5\MCF54A.seq
2 uL
1.0000 UG/kg
1
1.00
1.0000
Area Reject	J 0.00
Area Threshold : 100
Multiplier	: 0.68
Additive Constant: 0.00
Bunch Factor: 1
Instrument Conditions:
Capillary GC -
Instrument
Column
Column Length
Carrier Gas
Flow Rate
Split Ratio
Temperature
Injection Temp
Detector 1
Detector 2
Notes
VARIAN 3400
.23MM ID .25UMFILM RTX5
30M
HE
20CM/SEC LINEAR VELOCITY 15 PS I
160
200
300
1/MIN TO 230
Total Number of Peaks Detected: 49
EXTERNAL STANDARD REPORT
Ret Time	Component	Adjusted Amount Peak Area Peak Ht Raw Amount
[min]	Name	CuV-sec3 CuV]	ug\L
12.40 G-BHC	*	37.38 222941.00 12109.79	55.27
18.IS HPTCHLR	42.23 120340.00 6828.33	62.10
21.54 ALDRIN	39.35 248296.88 15326.87	57.87
27.04- MCPCPQX	0. 36	147Sr00	04. 58	0. 65 *>'
-50. 49 ENDQ1	0. 16	1792. 06	100. 61	0. 69	(f\\
33.92 DIELDRIN	126.44 264467.91 19356.97	183.93
D00330

-------
I
30¦ 23 END02	e*-38	1277.23	76.2*	0.D6 i/
41.10 CNDALD	2-r£3	2010i72	lQOiGl	2i9Q t-»
46.08 DDT	121.99 281975.13 24063.91	179.40 U
55.07 MCTIIOXV	:	3-^75	 2037. 00	143.71	5t54— ^
61.42 DBC	165.92 234651.00 18852.60	244.01
Total Area = 1382067.25
Total Concentration = 540.4901
Report by Doherty Bresnahan
000331

-------
rileHMt : C:\2700\GC5\HCF301SC.rin	Data: 8/29/89 9:53 AM Paga 1 1
Irt Tint 0.00 ain End Tiaai 70.00 ain Low Point: 5203 uV High Point: 33384 uV
tieal Scale Factor: 0.00 Plot Offset: 0 aV Plot Scale: 100 aV
Chroiatograa
1MH
* *5 a a* « ?s t i a3S3 anzsssn s* s s *. 63 sw C *
'• «•: : • 5 8 U Ma SUM MS* J 5 $ S P UK IS I 9
I
i
a.n~.
iusH
sur!
s.cH
_ I ii ii iiiL 11 irlrr i
i iiiiiihiii nVwrnrn
\ t I * £ § £ ! .
ii, i» i 11 i*. i i r. I1?, i f i r*i , i »|
Ir-i
11.(7	23.33	35.00	44.(7	5i33
Tis« (ain)
000332

-------
	Nelson Analytical 2700 Chromatography System Report Header
Sample Name : MS
Sample Numbers 9S185MS
Operator	s
T ime
Studv
8/29/89 2:04 PM
MCFARLAND
Inter-face #
AutoSampler
Rack/Vial
5	Channel
None attached
0/0
A/D mV Range
1000
Data Acquisition Times 8/29/39
Delay Time	: 0.00 min.
End Time	: 70.00 min.
Sampling Rate : 1.0 pts/sec
08 AM
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MCF5015C. raw
C:\2700\GC5\MCF5015I.rst
C:\2700\GCS\FOE.ins
C:\2700\GC5\EXSTD.pre
C: \2700\GC5-\MCF51B. smp
Cs\2700\GC5\MCF34B. seq
Ini. Volume
Sa.mp 1 e Amoun t
2 uL
1.0000 UG/kq
Area ft=.iect
0.0'.'
Noise Threshold
Dilution Factor
Divisor
1
1. 00
1.0000
Area Threshold
Mu11 i p1i er
Additive Constant
100
0.63
0.00
Bunch Factor
Instrument Conditionss
Cap i1lary GC -
Instrument
Column
Column Length
Carrier Gas
Flaw Pate
'5p 1 i t Rat io
T emperature
Injection Temp
Detector 1
Detector 2
Notes
3400
ID .25UMFILM RTX5
VARIAN
. 25MM
30M
HE
20CM/SEC LINEAR VELQCIT"
15 PS I
160
200
300
1/MN TO 230
Total Number o-f Peaks Detecteds 49
EXTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount
	L-V—
Peak Area
[u.V-sec 3
Peak Ht
CuV]
Raw Amount
u.q \L
101, 30
-fr-
-frH€	
		

—12Q0i 00
	01?. "0

13 ¦ uG

-shg	

a. 2i
1	
7e;

i
I
21.54
-59. 01.
ALDRIN
0 CHLD0NE
31.00 A CIILDAHC
41.72 243296.d8
0.-24	1166. 00
_0.IS 71G.OO
13326.37
	as.65
73. 31
6i.
000333

-------
34.61 DDE	81.96 357932.34 28188.66	120.53
36.76 ENDRIN	168.12 216304.22 16379.51	247.23 f
-40. 02 DDD	7.21	11229. 00	~29. 10	10. £0—
*4.03 CNDOGULrATC		6Q4. 99	71.24	0.30—
•51.31 CNDKCTO	7.-43	11269. 00	901: 46	10.91—^
61.42 DBC	210.79 234651.00 13852.60	309.99
otal Area = 1085732.00
otal Concentration = 518.7329
eport by Doherty Bresnahan
000334

-------
FileNaaa : C:\2700\GC3\nCF3015C.rui	Data: 8/29/99 2:03 PM Page I of 1
Start Tiaai 0.00 ain End Time: 70.00 ain Low Point! 5203 uV High Points 33384 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 #V Plot Scale: 100 aV
Chxcautograa
1N.W-:
aa-i
5I*K
» >xn a » s ssa asssss* :? ^ ^ s a
:• 8 It tx» R BR RMS? J 5 : ji ( !!« u I a
:«sH
i a
I
3
1 *
li
'IVrfS
< I	t
I
l~ff—I!!: :i ii iWi n niiniitnTHftrHrnn ; li'i ,i'n'i ii,in nfrm—-
m
j # i
¦ u ¦
1 H i? !
1 ,
I 3
, 'i
lit?
23.33 S.M
ii | i i i
1
tt.33
Til* (mia)
000335

-------
ID
PESTICIDE ORGANICS ANALYSIS DATA SHtET
tF'A SAMPLE NO.
QFOIDS PREGPC
Lab Name: LQCKHEED-ESC
Contract: 63-03-3249
Lab Code: 	 Case No. :
Matrix: (soil/water) SOIL
Sample wt/voi: 30 grams
Level: (low/med) LOW
Moisture: not dec. 1.9 dec.
Extraction: (SepF/Cont/Sonc)
SPC Cleanup: (V/N) N pH:
CAS NO.
COMPOUND
SAS No. :	SDS No. :
Lab Sample ID: 9S186DS
Lab File ID: 	
Date Received: 7-25-89
		Date Extracted:. 7-31-89
SONC	Date Analysed:
Dilution Factor:	10
CONCENTRATION UNITS:
ug/kg	Q
319-84-6	
31?-65-7	
3 1 ?-S6-5	
53-3?-®	
76-44-3	
309—00-2	
1024-57-3	
959-98-8	
60-57-1	
72-55-9	
72-20-8	
33213-65-9—
72-54-8	
1031-07-8—
72-43-5	
53494-70-5—
5103-71-9—
5103-74-2	
3001-35-2	
12674-11-2—
1 1 104-23-2-
11141-16-5-
53469-21-9-
12672-29-6-
11097-69-1-
11096-82-5-
-alpha-BHC	
-beta-BHC	
-de 1ta-BHC	
-gamma-BHC (Lindane;	
-Hep tach 1 or	.	
-A1dr in	
-Heptachlor epoxide	
-Endosul -fan I	
-Dieldr in	
-4,4'-DDE	
-Endr in	
-Endosul-f an II	
-4,4'-DDD	
-Endosul-fan suit ate	
-4,4'-DDT	
-Methoxycnlor	
-Endrin ketone	
-a1pha-Ch1 or dane	
-gamma-Ch1 ordane	
-T oxaphene	
-Aroclor-1016	
-Aroclor-1221	
-Aroclor-1232	
-Aroc1or-1242	
-Aroclor-1243	
-Aroclor-1254	
-Aroclor-1260	
o?
_/ ^
IJ
32
U
32
U
82
u
32
u
32
u
32
u
82
u
163
u
163
u
163
u
163
IJ
163
u
163
u
< t
IJ
315
IJ
163
u
32
•J
32
IJ
1631
u
315
u
315
¦J
315
IJ
315
u
815
u
1631
u
1631
u
FORM 1 PEST
1/37 Rev.
Q0033«

-------
Nelson Analytical 2700 Chromatography System Report Header
1:34 PM
Sample Name : OFOIDS Pre-GPC
Sample Number: 9S186DS
Operator :
Time
Study
8/30/89
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time : 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
3:23 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File
Sequence File
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFRO 21.raw
e:\pkd\MCFR021.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpa.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 UL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT*****
Instrument ID: Varian 3400-1
GC Column ID: 2250/2401
R«t IlM
Coopo&aac
Adjuatad Amount Raw Amount P«ak Araa Paak He MULTIPLIER
(min)
Na»
	
UG/L
[uV-««c)
[uVl
AdJ/Raw
3.31
G-BHC
• "60. M
39.01
2.38«ft
236136.32
0.68
4.32
HPTCHLR
63.28
96.00
2.38a«
188893.73
0.68
3.20
ALORIH
61 . 34
90.20
2.08«6
137333.34
3.68
11.20
0IELDRIH
261.69
384.84
3.32*6
223430.19
0.68
13.*9
END02
3.37
4. 96
139030.27
1300.43
0.68
17.36
00T
j. 7/ J2J. JJ." •
• 473.81
J.. 06«6
117049.33
0.68
23.61
DBC
219.71
323.10
-.10*6
76923.96
0.68
Total Area • 2310*884.00
Total Concentration ¦ 993.4631
Report by Tim Rand, Lockheed-ESC
A
000337

-------
Chromatogram
Filetfaae : e:\pkd\HCFR021.rau	Date: 8/30/09 1:14 PH Page 1 of 1
Start line: 0.00 ain End liae: 47.00 ain Low Point: 5920 uV High Point: 678230 uV
Vertical Scale factor: 0.00 Plot OffMt: 0 aV Plot Scale: 2S0 mV
CO
if*
250.000
208.333
166.667
125.000
IPTT,
-0.000	
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name : OFOIDS Pre-GPC
Sample Number: 9S186DS
Operator :
Time
Study
8/30/89 2:21 PM
MCFARLAND
Interface #
AutoSampler
Rack/vial
2	Channel : B A/D mV Range
Varian 8000 without controller
255/255
10000
Data Acquisition Time: 8/30/89
Delay Time	: 0.00 min.
End Time	: 47.00 min.
Sampling Rate : 1.0 pts/sec
3:23 AM
Raw Data File	:
Result File	:
Instrument File:
Process File	:
Sample File
Sequence File	:
Inj. Volume	:
Sample Amount	:
e:\pkd\MCFR0 21.raw
e:\pkd\MCFR021A.rst
e:\pkd\pkd.ins
e:\pkd\pextstd.pre
e:\pkd\clpb.smp
e:\pkd\MCFRLND.seq
2 uL
1.0000 uL
Area Reject
: 0.00
*****EXTERNAL STANDARD REPORT
Instrument ID: Varian 3400-1	GC Column ID: 2250/2401
R«t Tlaw
Caapoaarvt
Adju»t*4 Amount Raw Amount
Pailt Art*
P«»k Ht
MULTIPLIER
[mini
Nm».
UC/L
UC/L
[uV-s«e|
[uV]
AdJ/Raw
S.20
AL0KIN
57.03
83.89
2.08(6
157533.34
0.68
8.37
G-CHLDANE
0.32
0 . 1*7
961.0.00
351.58
0.68
11.20
DDE
283.36
417.01
3.32*6
225450.19
0.68
13.18
ENDUH
93.8*
138.00
1.91*6
68290.50
0.68
13.49
000
6.12
9.00
139030.27
3500.45
0.68
21.03
EHDOSULFATE
27.00
39.71
357933.00
3643.90
0.68
23.61
0BC
262.31
386.04
4.30*6
76923.96
0.68
Tool Ar*» - 17147396.00
Tool Concentration • 730.3897
Report by Tim Rand, Lockheed-ESC
00033??

-------
Chromatograra
FileNane : e:\pkd\MCFR02t.rau	Date: 8/30/69 2:22 PH Page t of t
Start Tlae: 0.00 ain End Tiae: 47.00 Bin Lou Point: 5920 uV High Point: 67B230 uV
Vertical Scale Factor: 0.00 Plot Offset: 0 nV Plot Scale: 250 raV
250.000
208.333
166.667
125.000
•0.000	
i r i
7.83	15.67	23.50	31.33	39.17
Time (min)

-------
Nelson Analytical 2700 Chromatography System Report Header
Sample Name
Sample Number
Operator
Inter-face #
AutoSampler
Rack/Vial
OFOIDS F'REGPC
9S136DS
5	Channel
None attached
O/O
T i me
Studv
9/1/39 2:26 AM
MCFARLAND
A/D mV Ranqe : 1000
Data Acquisition Time: 8/31/S9 11:04 FM
Delay Time
End Time
Sampling Rate
0.00
70.00
1.0
m in.
m in.
pts/sec
Raw Data File
Result File
Instrument File
Process File
Sample File
Sequence File
C:\2700\GC5\MC2010.raw
C:\2700\GC5\MC2010.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.pre
C:\2700\GC5\MCF2A.smp
C:\2700\GC5\MCF2CA.seq
[r, j. Volume
3 smp1e Arnounz
2 uL
1.00*50 UG/kq
A r & 3. P a j c
Noise Threshold
Dilution Factor
D ivi sor
1
1.00
1.0000
Area Threshold
Flu 11 i p 1 i er
Additive Constant
100
0. 63
0. 00
bunch Factor
Instrument Conditions:
Capillary GC -
Instrument
Co 1umn
Column Lanqth
Carrier Gas
Flow Pats
3clit Ratio
Temperature
I n .1 sc t i on Tamp .
Detector 1
Detector 2
Notes
VARIAN 3400
.25MM ID .25UMFILM RTX5
30M
HE
2CCM/SEC LINEAR VELOCITY 15 F":
160 1/M IN TO 230
200
300
Total Number o-f Peaks Detected: 49
EXTERNAL STANDARD REPORT
Ret Time
C m i n ]
Component
Name
Adjusted Amount Peak Area Pgak Ht Raw Amount
CuV-sec] CuVj	ug'^L
12.37 G-BHC
13. 13 HF'TCHLR
21.47 ALDRIN
30.jG CNOQl	
33.32 DIELDRIN
33.11 END02
14.67 73315.50 9932.13
63.83 191021.00 11819.32
56.34 239192.03 19006.17


204.
21.53
93. 37
C-®
'Wta i W ^
I

191.54 467115.72 36814.06
0.55 1378,.^110.06
3nr
231.67 /
0.81

-------
JgNDftLD
45.95 DDT
~ S. 7'?>—METHOX Y-
	*.11
206.90
—13. 2&
	S370.72
317112.00
6040.no
	*11.25-
28990.86
	456.11
	j i 0 0
304.26
19.80
318.45


2^
61.24 DBC
216.54 300420.00 25960.80
I
I
tal Area = 1657118.50
tal Concentration = 769.3851
sort by Doherty Bresnahan


-------
FileNut : C:\2700\GC3\HC2010.ra*	Date: 9/1/99 3:27 AH Page 1 of 1
Start Tinas 0.00 ain End Tines 70.00 tin Low Points 5214 uV Hi«h Points 51576 uV
Vertical Scale Factor: 0.00 Plot Offset: o mV Plot Scale: 100 «V
Chrasatograi
»* »

t !3 a*S=t« if,
fc OH*RMS :c
s?» *6 3
JrS fifi a
8
a
I si
l

TFT?i : i :r ;W^r~^nTfbfVflP'»i''i i'nin ;i; ;rnr
I * ^ - I a 3
1 | sj Sjjj
¦1 I ¦ ¦ I* I i'i I I I I r l"l I I- I fl
11.67	3.33	3.00	H.il
Time (ain)
«.33

-------
Nelson Analytical 2700 Chromatography System Report Header
| > mp1e Name : OFOIDS PREGPC
sample Number: 9S186DS
,per a tor	:
i
Time
Study
9/1/89 S:46 AM
MCFARLAND
iter-face #
AutoSampler
nek/Vial
I
5	Channel : A
None attached
0/0
A/D mV Range J 1000
?jita Acquisition Time: S/31/39 11:04 PM
Delay Time
Itd Time
amp ling Rate
Raw Data File
I3SUIt File
Tstrument File
Process File
iaiTio Is File
¦^queries File
0.00 m i n.
70.00 min.
1.0 pts/sec
C:\2700\GC5\MC2010.raw
C:\2700\GC3\MC201OA.rst
C:\2700\GC5\F0E.ins
C:\2700\GC5\EXSTD.prc
C:\2700\GC5\MCF2B.smo
C: \2700 v» G C 5\M C F 2 C 3. seg
I
riTiple Amount:
..oise Threshold
Dilution Factor
|„,o,
instrument Conditions:
t~sp i 11 ar y GC -
Instrument
Column
Column Length
C:. <.! 6
73.26
0.3?
-1r'r>
21.47 ALDRIN
20. "5" d-CHLDftNC
10.93 A-CHLDftNC
I
—

-------
34.50
36.65
DDE
ENDRIN
108.39 399391.23
221.52 363173.73
33363.35
28434.11
159.40
325.76
4





1
• CT 1 1 ¦
CMm/CTn
u•83 1338.uu
32. 34
1 .
1
61 . 24
DBC
220.90 300420.00
25960.30
324.85

Total Area = 1383602.50
Total Concentration = 620.4094
Report by Doherty Bresnahan


-------
! C:\2700\GC3\MC2010.ran
t Time: 0.00 ain End Tia»: 70.00 ain
ical Scale Factor: 0.00 Plat Offset:
DjU: 9/1/89 8U7 AH Paw 1 of 1
Low Paint: 5214 uV Hiah Paint: 51576 uV
0 aV Plat Scale: 100 aV
ChroMtograi
*6? I a«:n 2*
a; rn mm s8R K fS HRRRMS 55
lil
3
rp» fit. 3
s.»-
;».»-§
a
*-= 1
S
I 3
II!
11
•mi 11 ifi>ii irT^r"!roflrftTtor »i'i 'if.ji ;ii iVnr
11
? <£ 3 | 5 5 - 8 o § |	o
AM	Li	n 3,- 5 'm—I	r-L
11.67
23.33
35.00
Tia* (tin)
#>.U
38.33

-------