MIDWEST RESEARCH INSTITUTE*
                MRI
EPORT
STATIONARY SOURCE TESTING OF A MISSOURI-TYPE
            CHARCOAL KILN
          DRAFT
             DRAFT REPORT
            April 8, 1976
       Midwest Research Institute
      EPA Contract No. 68-02-1403
       MRI Project No. 3927-C(14)
                For

              Region VII
     Environmental Protection Agency
            1735 Baltimore
      Kansas City, Missouri 64108

      Attn:  Mr. Charles W. Whitmorc
      425 VOLKER BOULEVARD, KANSAS CITY, MISSOURI 64110 •  816561-0202

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MRI-NORTH STAR DIVISION 3100 38th Avenue South, Minneapolis, Minnesota 55406* 612 721-6373
MRI WASHINGTON, D.C. 20005- 1522 K STREET, N.W. • 202 293-3800

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                  STATIONARY SOURCE TESTING OF A MISSOURI-TYPE
                                 CHARCOAL KILN
                                       by
                               William H. Maxwell
                                  DRAFT REPORT
                                 April 8,  1976
                           Midwest Research Institute
                          EPA Contract No. 68-02-1403
                           MRI Project No. 3927-CC14)
                                      For

                                   Region VII
                       Environmental  Protection Agency
                                 1735  Baltimore
                          Kansas  City, Missouri  64108

                        Attn:  Mr. Charles  W.  Whitmore
MIDWEST RESEARCH INSTITUTE  425 VOLKER BOULEVARD, KANSAS CITY, MISSOURI 64110  •  816561-0202

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                             PREFACE






          The work reported herein was conducted by Midwest Research




 Institute (MRI) under Environmental Protection Agency (EPA) Contract




 No.  68-02-1403, Task No. 14.




          The project was under the technical supervision of Mr. Paul




 C. Constant,  Jr., Head,  Environmental Measurements Section of the Phys-




 ical Sciences Division.  Mr. William Maxwell served as project chief and




 was  assisted  by Mr. Bruce DaRos. The analysis of the samples was done




 by Dr. Clarence Haile, Ms. Carol Green, and Ms. Mary Woodfin under the




 technical supervision of Dr. Mark Marcus. Mr. Thomas Merrifield was re-




 sponsible for the data reduction and computer analysis. Some sample




 analysis was  done by Kansas City Testing Laboratories under the direc-




 tion of Mr. A. G. Cloud,  Chief Chemist.






 Approved for:




 MIDWEST RESEARCH INSTITUTE
 ^L/^7  Tfl
  —rrr^yv/
'.Paul C. Constant, Jr.
 Program Manager
         Av\-4Uvv^_
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                           TABLE OF CONTENTS
I.        Introduction• . 	 .....   1

II.       Summary and Discussion of Results 	   2

               A.  Mass and Total Organics.	   2
               B.  Polycyclic Organic Materials . . 	  10
               C.  Visible Emissions	•	14
               D.  Heat of Combustion	14

III.      Process Description and Operation .....  	  16

               A.  Process Description	16
               B.  Process Operation	19

IV.       Sampling and Analytical Procedures.  ....  	  21

               A.  Sampling	  21
               B.  Analysis	39

V.        Recommendations and Comments.	  42

References	44

Appendix A - Results of Analysis - Computer Computations  (Total
               Particulate) 	  45

Appendix B - Sample Calculations	71

Appendix C - Results of Analysis - Computer Computations  (Total
               Organic)	78

Appendix D - Results of Analysis - Computer Computations  (Poly-
               cyclic Organic Materials)	105

Appendix E - Flue Gas Combustion Computations	147

Appendix F - Computation of Kiln Volume	157
                                  iii

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                    TABLE OF CONTENTS  (Concluded)
Appendix G - Preliminary Runs - Field Data	162




Appendix H - Computation for Isokinetic Sampling	173




Appendix I - Table of Metric Equivalents	176







                            List of Tables




Table                            Title                            Page




  1       Summary of Particulate Results	    3




  2       Summary of Organic Results	    5




  3       Summary of Mass and Organic Data	  .  .    6




  4       Summary of Mass Emission Factors (Charcoal Production).    8




  5       Summary of Mass Emission Factors (Wood Utilization)  .  .    9




  6       Summary of ORSAT Results	•	•  •   11




  7       Summary of Polycyclic Organic Material Results	12




  8       Heats of Combustion	15




 A-l      Particulate Data and Calculated Values, Run 1	46




 A-2      Particulate Data and Calculated Values, Run 3 	   47




 A-3      Particulate Data and Calculated Values, Run 5 	   49




 A-4      Particulate Data and Calculated Values, Run 7 	   51




 A-5      Particulate Data and Calculated Values, Run 9 	   53




 A-6      Particulate Data and Calculated Values, Run 11	   55
                                  IV

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                      List of Tables  (Continued)




Table                            Title




 A-7      Particulate Data and Calculated Values,  Run  13	57




 A-8      Particulate Data and Calculated Values,  Run  14	58




 A-9      Particulate Emission Data	•   59




 A-10     Particulate Emission Data (Metric Results).  ......   62




 A-ll     Summary of Results (Particulate).	65




 A-12     Summary of Results—Metric Units (Particulate)	68




 C-l      Organic Data and Calculated Values,  Run  1	79




 C-2      Organic Data and Calculated Values,  Run  3  .	80




 C-3      Organic Data and Calculated Values,  Run  5	83




 C-4      Organic Data and Calculated Values,  Run  7  .......   85




 C-5      Organic Data and Calculated Values,  Run  9.......   87




 C-6      Organic Data and Calculated Values,  Run  11	89




 C-7      Organic Data and Calculated Values,  Run  13	91




 C-8      Organic Data and Calculated Values,  Run  14	92




 C-9      Organic Emission Data	   93




 C-10     Organic Emission Data (Metric  Results)	   96




 C-ll     Summary of Results (Organic).  .......  	   99




 C-12     Summary of Results—Metric Units (Organic)	102




 D-l      Benzfclphenanthrene Data and Calculated  Values, Run 2  .  106




 D-2      Benz[V]phenanthrene Data and Calculated  Values, Run 4  •  107

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                      List of Tables  (Continued)




Table                            Title




 D-3      Benz[cjphenanthrene Data and Calculated Values, Run 6 . 108




 D-4      Benz[£]phenanthrene Data and Calculated Values, Run 8 • 109




 D-5      BenzfVjphenanthrene Data and Calculated Values, Run 10. 110




 D-6      Benz[V]phenanthrene Data and Calculated Values, Run 12. Ill




 D-7      Benz[£]phenanthrene Emission Data	112




 D-8      Benz[^c]phenanthrene Emission Data (Metric Results). . • 114




 D-9      Summary of Results (BenzfVjphenanthrene)	116




 D-10     Summary of Results—Metric Units (Benz[cT]phenanthrene). 118




 D-ll     Benz[ja]pyrene Data and Calculated Values, Run 4 .... 120




 D-12     Benz[V]pyrene Data and Calculated Values, Run 6 .... 121




 D-13     Benz[_a]pyrene Data and Calculated Values, Run 8 .... 122




 D-14     Benz[V]pyrene Data and Calculated Values, Run 10. ... 123




 D-15     Benz[^a]pyrene Data and Calculated Values, Run 12. ... 124




 D-16     Benz[ai]pyrene Emission Data	 125




 D-17     Benz^ajpyrene Emission Data (Metric Results)	127




 D-18     Summary of Results (Benz[ja]pyrene).	129




 D-19     Summary of Results—Metric Units (Benz[V]pyrene). . • • 131




 D-20     POM-Like Material Data and Calculated Values, Run 2 . . 133




 D-21     POM-Like Material Data and Calculated Values, Run 4 . . 134




 D-22     POM-Like Material Data and Calculated Values, Run 6 . . 135




 D-23     POM-Like Material Data and Calculated Values, Run 8 . . 136
                                  VI

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Table




 D-24




 D-25




 D-26




 D-27




 D-28




 D-29




 G-l




 G-2




 G-3




 G-4




 G-5




 G-6




 G-7




 G-8
Figure




  1




  2





  3




  4
            List of Tables  (Concluded)




                       Title                            Page




POM-Like Material Data and Calculated Values,  Run 10. . 137




POM-Like Material Data and Calculated Values,  Run 12. . 138




POM-Like Material Emission Data 	 139




POM-Like Material Emission Data (Metric Results). ... 141




Summary of Results (POM-Like Material)	143




Summary of Results—Metric Units (POM-Like Material). . 145




Preliminary Data and Calculated Values, Run 1-P .... 163




Preliminary Data and Calculated Values, Run 2-P .... 164




Preliminary Data and Calculated Values, Run 3-P .... 165




Preliminary Data and Calculated Values, Run 4-P .... 166




Preliminary Data and Calculated Values, Run 5-P .... 167




Preliminary Data and Calculated Values, Run 6-P .... 168




Preliminary Emission Data 	 .......... 169




Preliminary Emission Data (Metric Results). 	 171







                  List of Figures




                       Title
The Missouri-Type Charcoal Kiln . .




Drawings of Sampled Kiln. . . . . .




Schedule of Burn and Testing Cycles
17




20




22
Preliminary Sampling Train A:  Runs Nos.  1-P and 2-P.  .   25
                                  vii

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                     List of Figures   (Concluded)




Figure                           Title




  5       Preliminary Sampling Train  B:   Run No. 3-P	27




  6       Preliminary Sampling Train  C:   Run No. 4-P	27




  7       Preliminary Sampling Train  D:   Run No. 5-P	33




  8       Preliminary Sampling Train  E:   Run No. 6-P	33




  9       Flammability Limits Apparatus  .....  	  37




  10      Cryogenic Sampling Apparatus	38
                                  viii

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                                NOTICE







           This  document  is  a  preliminary draft. It has not been formally




 released by EPA and  should  not  at  this  stage be construed to represent





 Agency policy.  It  is being  circulated for comment on its technical accur-





 acy and policy  implications.







                            I.   INTRODUCTION







           This  report presents  the results of source testing performed




 during the period  December  2  to 9, 1975, by MRI on a Missouri-type char-




 coal kiln at  the Wulff Charcoal Company, Vienna, Missouri. Testing for





 particulate,  total organic, and polycyclic organic material (POM) emis-




.sions  was conducted  on each of  the eight uncontrolled stacks of the kiln




 during a burn cycle,  a continuous  process.





           The testing was not done for  compliance reporting but rather





 for research  into  the general amount and types of emissions present dur-





 ing operation of a typical  kiln. The data are to be used for the possible




 establishment of new source emission standards and for evaluation of po-




 tential control  techniques  for  the charcoal industry in Missouri. The




 testing was also done as a  means of developing and evaluating source sam-




 pling  methodology  for charcoal kilns. The scope of work for this project




 specified:

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          1.  At least one sample per day for particulate,  total  organic,




and POM emissions over the period of a burn cycle.




          2.  Flammability limits sampling.




          3.  Visible emission observations.




          The following sections of this report present:




          1.  Summary and discussion of results;




          2.  Process description and operation;




          3.  Sampling and analytical procedures;  and




          4.  Recommendations and comments.







                II.  SUMMARY AND DISCUSSION OF RESULTS







A.  Mass and Total Organics




          Table 1 presents a summary of the particulate results for the




eight runs. Data are presented as grains per dry  standard cubic foot




(gr/dscf), milligrams per normal cubic meter (mg/ncm), pounds per hour




(Ib/hr), and kilograms per hour (kg/hr). Computer  printouts  of the field




data and reductions may be found in Appendix A. Sample calculations are




found in Appendix B.




          The runs are broken down into three sections. Run No. 1 was




completed during the 3-hr kiln start-up period before the doors were




closed and sealed. The resulting values may be considered representative




of emissions found during this period. They should only be considered

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                                               TABLE 1
                                 SUMMARY OF PARTIGULATE  RESULTS
Total particulate loadJL/
Run
No.


1

3
5
7
9
11
14

13
Partial^./
Date
Start-up

December
Burn-cycle
December
December
December
December
December
December
Other
December
gr/dscf£/ mg/ncm£/


2, 1975

3
4
5
6
7
8

8


1.09

0.36
0.76
CT- 95C^1
1.64
2.43
6.29

4.20


2,487

815
1,734
__6,751
3,745
5,553
14,383

9,602
Ib/hrcA

d/
ISO2-7

1.04
2.16
o • / 2
3.43
5.44
9.03

1.57
kg/hr£/

d/
82-

0.46
1.05
__— 3...0.6
1.55
2.46
4.10

0.71
To tali/
gr/dscf£' mg/ncm£/


1.32

0.80
2.21
<1
3.77
5.21
9.21

6.82


3,

1,
5,
39,
8,
11,
21,

15,


022

829
054
824
628
917
074

618
lb/hr£/

d/
219-

2.32
6.24
39.84
7.91
11.68
13.23

2.56
kg/hr£/

d/
99-

0.97
2.83
18.06
3.58
5.29
6.01

1.16
a/  Total for all stacks  emitting  during  test; 8 stacks for Runs Nos. 3, 5, 7, and 11; 7 stacks for
      Runs Nos. 9 and 14;  1.67  stacks  for Run No. 13; 1 stack (nominal) for Run No. 1; grains per dry
      standard cubic foot  and milligrams  per normal cubic meter are irrespective of number of stacks.
b/  Partial = Front half  of sampling train only (probe, cyclone, first filter)
    Total = Entire train
£/  gr/dscf = Grains per  dry standard  cubic foot
    tng/ncm = Milligrams per normal cubic  meter
    Ib/hr = Pounds emissions per hour
    kg/hr = Kilograms emissions per hour
d/  Values for Run No. 1  are approximate  and based on a nominal 10-ft diameter stack.

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approximate due to the sampling method as will be  reported later.  Runs





Nos. 3, 5, 7, 9, 11, and 14 are complete daily runs conducted each full





day of the burn cycle. These data indicate the trend of emissions  over





the cycle of the burn. Run No. 13 was a partial run covering  only  one





and two-thirds stacks on 1 day. These data may indicate those emissions





from a lesser number of stacks but were not used in subsequent emission





factor calculations.




          Sampling volumes for the six daily runs  varied from 16.80 dscf




(2.65 ncm) to 93.53 dscf (0.48 ncm). Values for the percent isokinetic





sampling rate varied from 94.0 to 104.6.




          Table 2 presents a summary of the organic results for the eight





runs. These data are based on the ether-chloroform extractable portion




of the particulate samples and are presented in the same form as the par-




ticulate data. Computer printouts of the field data and reductions are




found in Appendix C. The same raw field data and sample calculations as




for the particulate runs apply to the organic runs.




          The relationship between the total particulate catch and the




organic fraction is shown in Table 3. The emission rate from  the total





mass calculations is compared with that of the organic  fractions.  The




organic fraction of the total mass emissions is in the  range  of 66 to




77%.

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          TABLE 2
SUMMARY OF  ORGANIC RESULTS
                Total organic load£'
Run
No.
1

3
5
7
9
11
14

13
«/

b/

£/
Date
Start-up
December 2, 1975
Burn-cycle
December 3
December 4
December 5
December 6
December 7
December 8
Other
December 8
Total for all stacks
Runs Nos. 9 and 14;
standard cubic foot
Partial = Front half
Total = Entire train
gr/dscf = Grains per
Partial^/
TotalJi/
gr/dscf£/ mg/ncm£/ lb/hr£/ kg/hr£/
0.77 1,755 127-

0.30 593
0.60 1,372

1.26 2,875
1.92 4,390
4.50 10,300

2.70 6,169
emitting during test; 8
1.67 stacks for Run No

0.72
1.68

2.66
4.32
6.44

1.02
stacks
. 13; 1
SB*/

0.34
0.79

1.19
2.71
2.94

0.46
gr/dscf£/ mg/ncn£A
0.89

0.55
1.62
13. 45
2.86
3.54
6.38

4.52
for Runs Nos. 3
stack (nominal)
and milligrams per normal cubic meter
of sampling train only

dry standard cubic foot
(probe,


cyclone,


2,

1,
3,
30,
6,
8,
14,

10,
045

269
718
782
535
105
608

334
,5, 7, and
for Run No.
are irrespective of
first


filter)





lb/hr£/
148^

1
4
30
6
8
9

1

.60
.56
.80
,535
,105
.17

.68
kg/hr£/
67^

0
2
13
1
3
4

0

.73
.08
.95
.94
.59
.17

.77
11; 7 stacks for
1; grains per dry
number of






stacks.






mg/ncm = Milligrams per normal cubic meter
Ib/hr — Pounds emissions per hour
kg/hr = Kilograms emissions per hour
±1
Values for Run No. 1
are approximate and based on a
nominal
10-ft diameter
stack.

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             TABLE 3
SUMMARY OF MASS AND ORGANIC DATA
Run
No.

1

3
5
7
9
11
14

13
£/


b/
Total
Date
Start-up
December
Burn-cycle
December
December
December
December
December
December
Other
December
lb/hrb/

2,

3
4
5
6
7
8

8
Total for all
5, 7, and 11
No. 13; 1
train.


1975 219s-'

2
6
39
7
11
13

2

.32
.24
.84
.91
.68
.23

.56
ma ss ay
Total
organic^/
kg/hrb/ lb/hrb/ kg/hrb/

99£/

0.97
2.83
18.06
3.58
5.29
6.01

1.16
stacks emitting during
; 7 stacks for Runs Nos
stack (nominal)

Ib/hr = Pounds

emissions

per
kg/hr = Kilograms emissions
£/
Values for
Run
No. 1 are




c/ c/
149s-' 67-

1
4
30
5
7
9

1

.60
.56
.80
.95
.92
.17

.68
test; 8
. 9 and
for Run No. 1;

hour
per hour
approximate




0
2
13
1
3

.73
.08
.95
.94
.59
4.17

0
stacks
14; 1.
data is






and based on a

.77
Percent
organic

68

69
73
77
75
68
69

66













for Runs Nos. 3,
67 stacks for Run
for



entire sampling



nominal 10-ft



di-
ameter stack.

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          Table 4 presents a summary of the mass emission factors (unit





emissions per unit charcoal produced) for each run as well as the total





for the burn cycle. These emission factors have been computed by three





methods. In the first method, the data for each run are taken to repre-





sent that of the 24-hr period encompassing the run time. The data for





the 3-hr start-up period are added to form the total emission factor for





the burn cycle. This method does not include the shut-down period of the




cycle. The second method utilizes the data from each run as representa-




tive of the emissions over a 28-hr period around each sample time. This




method includes the start-up and shut-down periods. The last method takes





the data from each run as being consistent with that of a 27.5-hr period





around each sample time. The data for the start-up period are added to





form the total while the shut-down period is included. These methods




yield total emission factors ranging from 126.4 to 160.5 Ib of emissions




per ton of charcoal produced (63.2 to 80.2 kg of emissions per metric




ton of charcoal produced).





          Table 5 presents the same data but figured as unit emissions




per unit wood used in the charcoal production. The data were computed




by the same three methods as that for Table 4. The results range from




26.8 to 34.1 Ib emissions per ton wood utilized (13.4 to 17.0 kg emis-




sions per metric ton wood utilized).

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                                                                                 TABLE  4
                                               SUMMARY  OF MASS  EMISSION FACTORS  (CHARCOAL  PRODUCTION)
00
Run
No.'
IS/
3
5
7
9
11
14
Total
METHOD I3'
METHOD IlJi/
Total mass Total mass
Period emissions Emission factor Period emissions Emission factor
covered lb£f kg£/ lb/tonfi/
n lTTl975 656 298 36'5
December 2, 1975
1540 December 2
1540 December 3 " " 3'1
1540 December 3 ^ 6g fl>3
1540 December 4
1540 December 4
1540 December 5
fstn n^" * 19° 86 10-5
1540 December 6
1540 December 6 28Q
1540 December 7
1540 December 7
1540 December 8 318 144 17'6
147 hr 2,606 1,181 144.7
METHOD IIl£/
Total mass
Period emissions Emission factor
kg/MtonS/ covered lb£/ kg2' Ib/tonS/ kg/Mton£/ covered Ibl/ kgg/ lb/ton£'
IS. 2
1240 December 2
1640 December 3
4.2 "*9 DeCe^er ' 175 79 9.7 4.9
2040 December 4
26 -5 nn?n DCCe°ter « M" 506 62.0 31.0
0040 December 6
5-3 rnDeCeter? "1 10° 12'3 6.1
0440 December 7
0440 December 7
7'8 0840 December 8 327 l48 18'2 9>1
8.8 0840 December 8 2Q
1240 December 9
72.3 168 hr 2,274 1,030 126.4 63.2
656 298 36.5
December 2, 1975
1540 December 2 0
1910 December 3 6* 29 3'5
1910 December 3 UJ ?g ,_5
2240 December 4
2240 December 4
0210 December 6
0210 December 6
0540 December 7
0540 December 7
0910 December 8 321 U5 l7'8
?9ln neCe"ter S 3" l" 20.2
1240 December 9
168 hr 2,891 1,311 160.5
kg/Mtonl/
18.2
1.8
4.8
tCSP
"^gttBmiG
JO^
8.9 KjeaCTBKB
tt^|
80.2
            a/  Based on 24-hr periods per run plus 3 hr start-up; excludes shutdown.
            b/  Based on 28-hr periods per run including start-up and shutdown periods*
            c/  Based on 27.5-hr periods per run plus 3 hr start-up; includes shutdown*
            d/  lb = Pounds emissions
               kg — Kilograms emissions
               Ib/ton = Pounds emissions per ton charcoal produced (based on 18 tons charcoal)
               kg/Mton = Kilograms emissions per metric ton charcoal produced (based on 16.33 Mtons charcoal)
            cl  Values Cor Run No. I are approximate.

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                                                                                     TABLE 5
                                                     SUMMARY OF  MASS EMISSION  FACTORS  (WOOD  UTILIZATION)
                                                                                        METHOD
                                                                                               Tb/
                                                                                                                                          METHOD III-'
VO
Run
No.
*
3
5
7
9
11
14
Total
Period
covered
1240-1540
December 2, 1975
1540 December 2
1540 December 3
1540 December 3
1540 December 4
1540 December 4
1540 December 5
1540 December 5
1540 December 6
1540 December 6
1540 December 7
1540 December 7
1540 December 8
147 hr
Total mass
emissions
Ibl/ ka°/
656 298
56 25
150 68
956 433
190 86
280 127
318 144
2,606 1,181
Emission
lb/ton£' t
7.7
0.7
1.8
11.3
2.2
3.3
3.7
30.7
factor
ig/Htong/
3.9
0.3
0.9
5.6
1.1
1.6
1.9
15.3
Period
covered

1240 December 2
1640 December 3
1640 December 3
2040 December 4
2040 December 4
0040 December 6
0040 December 6
0440 December 7
0440 December 7
0840 December 8
0840 December 8
1240 December 9
168 hr
Total mass
emissions Emission factor
~"°" ~&S~ °"~ "^
65 29 0.8 0.4
175 79 2.1 1.0
1,116 506 13.1 6.6
221 100 2.6 1.3
327 148 3.8 1.9
370 168 4.4 2.2
2,274 1,030 26.8 13.4
Period
covered
1240-1540
December 2, 1975
1540 December 2
1910 December 3
1910 December 3
2240 December 4
2240 December 4
0210 December 6
0210 December 6
0540 December 7
0540 December 7
0910 December 8
0910 December 8
1240 December 9
168 hr
Total mass
emissions
Ibi'
656
64
172
1,096
218
321
364
2,891
298
29
78
497
99
145
165
1,311
Emission
Ib/toni' I
7.7
0.8
2.0
12.9
2.6
3.8
4.3
34.1
factor
cg/Mtoi^d/
3.9
0.4
^
6.4 ||l|™
K3
U9 sagg
2.1 «HaBi
17.0
              a/  Based on 24-hr periods  per run plus 3 hr start-up; excludes  shutdown.
              b/  Based on 28-hr periods  per run including start-up and shutdown periods*
              £/  Based on 27.5-hr periods per run plus 3 hr start-up; includes shutdown.
              d/  Ib = Pounds emissions
                 kg = Kilograms emissions
                 Ib/ton = Pounds emissions per ton wood utilized (based on 84.96 tons wood)
                 kg/Mton = Kilograms emissions per metric ton wood utilized (based on 77.07 Mtons wood)
              el  Values for Run No. I are approximate.

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          Table 6 presents a summary of the ORSAT results  for the  stack





gas compositions. Values for the percent by volume of carbon monoxide





and carbon dioxide generally increased over the period of  the burn while





that for oxygen generally decreased. These values may be in error  some-





what due to the presence of volatile hydrocarbons in the gas stream, but





are thought to be representative.





          Percent moisture values ranged from 25.5 to 35%  (by volume)  for




the six daily runs. These values are at or slightly below  moisture satu-




ration. The value for the volume of water collected was back-calculated




using the standard equation for those runs at moisture saturation  (these




values were needed for entry with the computer program). The value for





Ap at each point found in the computer printouts was back-calculated from




the input velocity data, since no direct Ap readings were  obtained by





pitot readings due to the low flow. These values are shown merely  to in-




dicate approximate readings that would be expected.







B.  Polycyclic Organic Materials





          Table 7 presents a summary of the POM results for the  six runs.




Data are presented as for the mass and total organics. Computer  printouts





of the field data and reductions may be found in Appendix  D. The sample




calculations are the same as for the mass data.
                                  10

-------
                                          TABLE  6
                                SUMMARY OF ORSAT RESULTS
     Date




December 3, 1975
December 4, 1975
December 5, 1975
December 6, 1975
December 7, 1975
December 8, 1975
Percent by volume
Stack



Average


Average



Average


Average



Average


Average
14)
7
3
5
(Runs
5
8
(Runs
6
2
8
(Runs
7
7
(Runs
4
8
6
(Runs
8
1
(Runs

Time
1000
1255
1530
Nos. 1, 2, 3)
0900
1230
Nos. 4, 5)
0830
1200
1400
Nos. 6, 7)
0900
1030
Nos. 8, 9)
0940
1130
1300
Nos. 10, 11)
0900
1300
Nos. 12, 13,

C02
9.80
8.67
14.40
10.96
17.00
13.00
15.00
12.67
12.27
26.73
17.22
14.60
17.53
16.07
22.17
21.00
11.40
18.19
22.67
22.00
22.33

02
10
11
5
9
6
7
7
8
11
7
9
7
4
6
2
2
10
5
0
1
1

.67
.53
.33
.17
.87
.73
.30
.53
.73
.40
.22
.93
.87
.40
.37
.40
.60
.12
.87
.40
.13

CO
1
1
2
1
4
1
2
2
2
7
4
1
1
1
7
6
3
5
8
5
6

.73
.73
.20
.88
.00
.87
.93
.53
.60
.27
.13
.33
.67
.50
.07
.40
.00
.49
.20
.13
.67

Molecular weight
dry stack gas
N2
77
78
78
77
72
77
74
76
73
58
69
76
75
76
68
70
75
71
68
71
69

.80
.07
.07
.98
.13
.40
.77
.27
.40
.60
.42
.13
.93
.03
.40
.20
.00
.20
.27
.47
.87

(Ib/lb-mole)
29
29
30
30
30
30
30
30
30
32
31
30
31
30
31
31
30
31
31
31
31

.99
.85
.52
.12
.99
.39
.69
.37
.43
.57
.12
.65
.00
83
.64
.46
.25
.12
.66
.58
.62


-------
                                                TABLE  7
                  SUMMARY  OF  POLYCYCLIC ORGANIC  MATERIAL RESULTS
Total POM load!i/
Run
No. Date
Bum-cycle
2 December 3, 1975

4 December 4


6 December 5


8 December 6


10 December 7


12 December 8


POM
material^

1
2
3
1
2
3
I
2
3
1
2
3
1
2
3
1
2
3

' Kr/dacf£/
15.2
NDS/
339.7
3.3
3.3
137.8
12.4
3.6
77.9
ND
ND
ND
ND
ND
197.3
ND
ND
837.0
Partial^./
iPR/ncmj/
34.7
ND
777.3
7.5
7.5
315.3
28.4
8.3
178.3
ND
ND
ND
ND
ND
451.6
ND
ND
1,915.4
Ib/nrg/
44.2
ND
989.3
9.4
9.4
394.6
27.6
8.0
173.1
ND
ND
ND
ND
ND
383.8
ND
ND
1,194.7
kg/hd/
20.0
ND
448.7
4.2
4.2
179.0
12.6
3.7
78.6
ND
ND
ND
ND
ND
174.1
ND
ND
541.9
Sr/dscf*/
15.2
ND
370.2
22.6
13.8
205.3
12.4
8.1
118.6
26.7
8.9
257.3
12.7
20.7
513.8
51.0
60.2
1,485.3
Totalf./
-Efi/ncma/
34.7
ND
847.2
51.6
31.5
469.7
28.4
18.6
271.4
61.0
20.3
588.7
29.1
47.4
1,174.1
116.7
137.7
3,399.0
tb/hd./
44.2
ND
1,078.2
64.6
39.4
587.8
27.6
18.1
263.5
55.9
18.6
538.7
24.7
40.3
997.8
72.8
85.9
2,120.0
kg/hd/
20.0
ND
489.0
29.3
17.9
266.6
12.6
8.2
119.5
25.3
8.5
244.4
11.2
18.2
452.6
33.0
38.9
961.7
al  1 = Benz[cjphenanthrene
    2 — Benz[ji]pyrene
    3 = POM-like material
    All other POM's not detectable.
b_/  Total for all stacks emitting during tests} 8 stacks for Runs Nos* 2,  4,  6, and 10; 7 stacks for  Runs Nos. 8
      and 12; grains per dry standard cubic feet and milligrams per normal cubic meters irrespective  of number
      of stacks.
£/  Partial = Front half of sampling train only (probe, first filter)
    Total = Entire train
d/  gr/dscf = Grains per dry standard cubic foot x 10
    mg/ncm = Milligrams per normal cubic meters x 10
    Ib/hr = Pounds emissions per hour x 10"**
    kg/hr — Kilograms emissions per hour x 10
e/  ND = Not detectable.
«-6

-------
          The six sets of samples were analyzed for the following POMs:




          Benz[£]phenanthrene




          Benz[_a]pyrene




          Dibenz|ja,hJ anthracene




          3-Methylcholanthrene




          7,12-Dimethylbenz[ja]anthracene




          3,4,5,6-Dibenzocarbazole




          Other materials found on the chromatograms were classified as




POM-like materials. These were defined as the total of unassigned peaks




eluting after 3-methylcholanthrene, and may reflect the degree of clean-




up. They were classed together and reported like the other POMs. Detect-




able quantities were found only for benz[cjphenanthrene, benz[_a]pyrene,




and the POM-like material. Quantities for the other POMs, if present,




were below the detection limits for the given sample volumes. The ranges




of the detection limits for the various POMs were as follows:




            Benz[c_]phenanthrene:  1.2 to 4.1 |j,g/sample




            Benz[ajpyrene:  1.0 to 2.0 |j,g/sample




            Dibenz^,hjanthracene:  1.5 to 4.5 y,g/sample




            3-Dimethylcholanthrene:  0.4 to 0.8 ng/sample




            7,12-Dimethylbenz[ji]anthracene:  1.0 to 2.0 jig/sample




            3,4,5,6-Dibenzocarbazole:  4.0 to 10.0 p,g/sample
                                  13

-------
G.  Visible Emissions





          Observations of the visible emissions according to procedures





established in EPA's Method 9-  were not made. However,  frequent  obser-





vation of the stacks by two trained, but not currently certified,  obser-





vers indicated that the opacity was seldom,  if ever,  lower than 100%.  As





compliance testing was not involved, it is felt that  these observations





are valid as indicators of the general state of the visible emissions





from an operating charcoal kiln.




          As the stack gas was at or near moisture saturation,  some  steam




may be included in the visible emissions, causing problems with the  read-




ings. The plumes of the several stacks and kilns readily mingle,  making





readings from any one stack difficult at times.







D.  Heat of Combustion




          Table 8 presents a summary of the heat of combustion  data  for




the five cryogenic samples. The heat of combustion values are given  for




both the water and tar and oil fractions as  recovered from the  sampling




apparatus. The heats of vaporization given are for the amounts  of water




collected. The net heat available from the flue gas stream is found  by





summing the heats of combustion for each sample and subtracting the  re-




spective heats of vaporization. The air/fuel ratios are approximate  val-





ues for the volume of air per unit volume of flue gas needed for  stoi-




chiometric combustion of the flue gas. The stoichiometric heat  indicates
                                  14

-------
                                                           TABLE 8
                                                    HEATS OF COMBUSTION
Volume
flue gas
sampled Sample
Dace (cf)£/ No.
December 4, 19752/ 0.84 1-1
1-2
-a.—- December &J 0.94 2-1
^^^jH 7-9
:*s&
HSI t-' December 1- 1.88 3-1
"•ISSP Ui 10
i*^8* December 8^ 2.57 4-1

-------
the quantity of heat required to combust the flue gas stream and added



air under stoichiometric conditions. The negative values indicate that



an additional fuel source must be provided as the flue gas stream will



not sustain combustion of itself. Additional information may be found



in Appendix E.





               III.  PROCESS DESCRIPTION AND OPERATION





A»  Process Description



          Charcoal in Missouri is manufactured by means of the pyrolysis,


                                                               2-4/
or destructive distillation of wood, utilizing the kiln method.	  The



wood is heated in generally air tight ovens using controlled amounts of



air. Wood moisture, volatiles, and combustion gases are driven off by .



the high temperatures generated. Combustion of part of the wood volatiles



produces heat to sustain the carbonization process. The waste gases  are



emitted to the atmosphere through the kiln stacks leaving a product  of



highly carbonized charcoal, along with some partially charred wood which



may be used in subsequent kiln loadings. Approximately 4,000 Ib (1,814



kg) of wood must be used to obtain 1,000 Ib (454 kg) charcoal.



          A typical Missouri-type kiln is shown in Figure 1. Wood is



loaded through the door and the roof ventilation ports leaving some  air



space along the bottom of the kiln. The fire is usually started at the



bottom center of the kiln using kindling or other easily combustible ma-



terials placed there during loading. During the start-up phase,  the  door
                                  16

-------
             •Clay  Sewer
             Pipe Stacks —
                                                     Roof Ventilation
                                                     Ports
Air Pipes
       Steel Doors —
Concrete Walls
and  Roof
                     Figure 1 - The  Missouri-Type Charcoal Kiln

-------
and roof ventilation ports are left open. The ports are closed first





after approximately 1 hr and then the doors are closed after  2 to  3 hr.





Combustion air inflow is then provided through the use of air pipes near





the floor and controlled to prevent complete ashing of the wood* Stack





gas velocities are only slightly greater than natural  convection and





may cease altogether at times in any given stack,  depending on the loca-





tion of hot spots in the kiln, and wind direction  and  velocity. Generally,




the burn is completed when the fire has reached the floor of  the kiln,





having burned from top to bottom and center to walls.  At this time, all





openings are sealed off, preventing further air inflow or waste gas emis-




sion, killing the fire, and allowing the kiln to cool.





          Burn times vary with the type and size of kiln,  operator ex-





perience and practice, the type of wood used, and  the  degree  of carbon-




ization or quality of product desired. A typical cycle may be within  the




time frames given below:




          1-2 days to load;




          5-8 days to burn;




          10-14 days to cool; and




          1-2 days to unload.




          The kilns are generally of concrete construction and may have




exposed walls or earthen embankments to provide insulation. Stacks may




be constructed of many materials but are usually of 6  to 8 in. (15.2  to
                                  18

-------
20.3 cm) diameter clay sewer pipe with water pipe and galvanized stove





pipe also being used. Stack heights may vary from kiln to kiln or among





stacks of a given kiln. No emission control devices are known to be in





operation in Missouri on Missouri-type kilns.







B.  Process Operation




          The kiln tested at the Wulff Charcoal Company, Vienna,





Missouri, operates as a typical Missouri-type charcoal kiln.  Drawings




of the kiln are presented in Figure 2. The kiln has been in operation





for 25 to 30 years. The wood utilized is generally white (post) oak,




and may be either fresh cut cordwood, aged (dried) cordwood,  or sawmill





waste bark-edge slabwood. Prior to this test series, the kiln owner had




several truck loads of the various wood types measured and.weighed to




obtain an average pounds per cubic foot (pcf) value for the wood used




in this test kiln. This value is probably very representative as the




wood is stacked as tightly in the kiln as it is on the truck. The aver-




age value obtained was 29.5 pcf (472.5 kg/cu m). Thus, this kiln has a




capacity of approximately 191,300 Ib (86,790 kg) or 50.5 cords of wood.




Calculations relating to the kiln volume are found in Appendix F. Allow-




ing for air space left around the walls and roof and provided on the




floor, the usable wood volume would be approximately 45 cords (169,920





Ib, 77,074 kg), which will be used as the capacity for this test. As




most of the charcoal produced by Wulff Charcoal is used for industrial
                                  19

-------
  Earth
N
   Air

   Pipes
Concrete -
  Earth

—





i
— *
-r*
\




^




:-
r:
•

i



~-e o ir-
61" 100" 94" . 1(

POO

Roof Ventilation
O— -rp — O.
r £
O 0 i
o o'
•—12" 384" (32')

! ! I ' J !
O o O

56" 100" 97" 10

W1

(

Cf~
- Do
>
^
*i

1
c

2"

"i i

•}

.
cl
or
)
,
j
)

53
n





L
X
\






\
7



7

12
7

i
41



2"



2"

0" T-
-I
,
'

-







'
io
0







N
• i

^>^'\ r\6" '-D-
JL//^ ^xxt \.
! 6" 1 |i Hi
i lii,1
— ^ i i P 'i
ik i ' ' i
"^ , 1 1 i n
— .in
^ IN it
00 | ' II |l|
!' 1 urn mm 1 !! ill
/ \
<— Air Pipes— ^
b. ELEVATION

                                                                                                                  D. Clay Sewer Pipe
                             a. PLAN
         Stack No.5
Stack No.  4


•n
i
i
! C 45" 1 43^~ |
f * rf i r
1 1 i
!' '
1 i
ii
u
!!
n
n
n
f3 ^H"
• t "
i ? II
i n
i|
,i
                                                            . Steel
                                                           Air Pipes
                                                                           4
                                                                             -i
          '   T
          |i 24"

          !i
                                                                                              20" |

                                                                                                  il
                                                                                                  u
II  t
U 20"
II
II
I'



L
                          c. SOUTH SIDE
                                              ( 1 ) Not to Scale

                                              (2) All Measurements  Approximate

                                                  Due to Surface Irregularities
                                                                                      d. NORTH SIDE
                                       Figure  2  - Drawings of Sampled Kiln

-------
purposes, they try to obtain a higher degree of carbonization than is





normal. This also yields a lower amount of charcoal per cord of wood





than is normal, only around 800 lb (363 kg) charcoal per cord. Thus,





the charcoal production of the kiln for this test would be approximately




36,000 lb (16,330 kg).





          The kiln was loaded and ready to be lit by noon, Tuesday,





December 2, 1975. Figure 3 presents a comparison of the kiln burn cycle




with the sampling test cycles. At first, the closed door was not completely





sealed but gradually the kiln was sealed such that only the air pipes




and exhaust stacks remained open. Close-down began on the afternoon of




Monday, December 8, 1975, with the sealing of two exhaust stacks and was




completed by approximately noon, Tuesday,  December 9, 1975, yielding a




7-day burn cycle.







               IV.  SAMPLING AND ANALYTICAL PROCEDURES







A.  Sampling





          Due to the nature of the charcoal kiln itself and the types




of materials emitted in the waste gas stream, in addition to the general




lack of information relating to the testing of a kiln during operation,




a portion of the task was to evolve a sampling train and technique that




would handle the effluent constituents with reasonable case.




          Various sampling techniques were examined for use on the proj-




ect. One was to sample each emitting stack each day. This would yield up
                                  21

-------
     DATE
             00
2 December 1975
(Tues)

3 December 1975
(Wed)
4 December 1975
.(Thur)
5 December 1975
(Fri)
6 December 1975
(Sot)
7 December 1975
(Sun)
8 December  1975
(Mon)
9 December 1975
(Toes)

00 06

Run 1
Run 3
Run 2

Run 5
Run 4

Run 7
Run 6

Run 9
Run 8

Run 11
Run 10

Run 13
Run 14
Run 12


Tl/
00 12


a oa a
A A 6
o
a o a a
A A A A
O
a a a a

O (
a a aa a
A A AAA
0 O
a a aa a
A AAA AA
O O
a a
am
A A AA
O

V\E
00 18
1240 1540
a a
ao o a a a
A A A A A
0 0
a o a a
A A A A
O •
a a a a

1 O
a a
A A
*
aa a
A A
o •

i acorn
A AA
o v ••
1240

00 24






















                                                                          00
    a
    A
    o
Kiln Start-up
Burn Cycle
Kiln Close-down
Parti cu late-Organic
POM (5 min sample)
Orsat (grab sample)
Cryogenic sample
           Figure 3  -  Schedule of Burn and Testing Cycles
                                      22

-------
to eight samples per day. However, as the proper recovery of samples is




time consuming, this method of sampling would not be practical for use




during 1 day. Another technique would be to composite several stacks into




one sample, yielding one to four samples per day. By compositing samples




from all emitting stacks into one daily sample,  a closer compromise be-




tween the task objectives and an amount of work  that could reasonably be




done in 1 day could be achieved. Thus, it was decided to sample each emit-




ting stack once per day, compositing the samples together for one sample




or run per day. Each stack would be sampled for  the same amount of time




on a given day.




          In order to do the actual testing,  basically two train config-




urations were considered. The first method would involve manifolding the




stacks together and sampling the common duct. This method would involve




considerable problems in material deposition in  the manifold ducting and




possible disruption of the normal operation of the kiln or the natural




draft of the stacks. It was rejected in favor of the other method. By




sampling each emitting stack in turn with the same sampling apparatus




without sample cleanup between stacks, samples from the individual stacks




would be automatically combined for a daily average. It was felt that by




using this sampling method and by modifying the  standard EPA Method 5




sampling train,—  a workable system would result.
                                  23

-------
          1.  Mass and total organics





               a.  Preliminary tests;  As tars  and oils,  present  in  the





waste gas stream, were predicted to plug a glass-fiber  filter  easily,





the filter was moved from its normal position at  the  front  of  the train





to the rear, just ahead of the silica gel (Figure 4). Also,  as the pres-





ence of polycyclic organic matter (POM) in the  effluent  stream was being





investigated, 2% sodium carbonate was substituted for distilled water  in




the first two impingers due to the greater solubility of  POMs  in  sodium





carbonate. No probe or filter heaters were used.  As the  stack  gas flow





rate was very low, glass tubing of approximately  0.5  in.  (1.3  cm) ID was





used as a probe and probe tip.




               To check out this train and related sampling procedures,




as well as the analytical techniques, a preliminary series  of  tests  was




conducted at a kiln operated by Noblett Charcoal, Belle,  Missouri. Two





1/2-hr tests (Runs Nos. 1-P and 2-P) were run on  one  stack  of  the kiln




during a burn cycle. The impingers were maintained in an  ice water bath.




Stack gas temperatures were obtained using a thermocouple and  potentio-




meter while stack gas velocities were measured  with a Type  3002-2G Alnor




Velometer. The velocities were too low for accurate reading using the




standard Type-S pitot tube. The velometer presents problems as it is sus-




ceptible to ambient wind and possible internal  interference due to oil





and tar entrained in the flue gas stream. Sampling was  done at a  constant,
                                  24

-------
T
     f
      o
     0
                                                •Glass Fiber Filter

t
t



\
\

\

i
j


:

i
t

,



j
_j


;



.

\
m
i w
T
^


                                                         -4V-
V_?% <;«,«, im     V.
   x»———^       I  \ vr       yf ..i      i.i. a.j          *
  _*j    |*_~6"  ^---\ — -/---	^^Ar	
                                             Metering
                                             Console
                             Sodium
                         Carbonate
-Silica Gel
    Figure 4 - Preliminary Sampling Train A:   Run Nos. 1-P and 2-P

-------
low flow rate of approximately 0.25 actual cubic feet per minute (0.007





actual cubic meters per minute). One flue gas determination by ORSAT





analysis was conducted. Moisture determinations were made using the





volume of collected water. The probe tip projected into the stack ap-





proximately 6 in. (15.3 cm) directly from the top. It was not practice-





able to establish ports in the stack and extensions were not used in




order to disturb the stack draft characteristics as little as possible.




Also, no traversing of the stack was done due to the large probe tip




size with respect to the small stack size. No general problems were en-




countered during sampling with this train.





               As difficulties arose in the analysis of the samples of





the first preliminary series, a second preliminary series of testing




was done at Wulff Charcoal, Vienna, Missouri. In this series, four train




variations were examined, two for the mass and organic analysis and two




for the POM analysis, to be examined later. For the mass-organic trains,




the standard EPA Method 5 sampling train was used with the inclusion of





a filter prior to the silica gel (Figures 5 and 6). The first test (Run




No. 3-P) was done with both train filters at atmospheric temperature




while the second test (Run No. 4-P) was run with the first train filter




heated to approximately 350°F (177°C).




               Due to the high moisture content of the flue gas (~ 30%




by volume), a considerable amount of water was condensed onto the un-




heated first filter during Run No. 3-P, filling perhaps one-third the
                                  26

-------
/
                                          Glass Fiber Filter
r
                                                Glass Fiber Filter
                        6n
f
                            O
                           O
   T,  X     X  I     1   f"^"^  I
    T   i      *P  *r     TT        TT
                              /-Stack
  i*—6"
                                                   Distilled
                                                   Water
                     Metering
                     Console
                                              •Ice Bath

                                          -Silica Gel
ISi
                                  Figure 5 - Preliminary Sampling  Train B:  Run No.  3-P
                                           'Glass Fiber Filter
                                                 Glass Fiber Filter
                          *
                           IA
                           a
                          0
                                     i jjj
                              -»—»p>
                               350
                               -Stack
                         Distilled
                         Water
                                            Silica Gel
                                  Figure 6 - Preliminary Sampling  Train C:  Run No.  4-P

-------
volume of the filter holder. The second filter had no observable mate-





rial on it after 30-min running time. It is believed that the wet first





filter acted as scrubber or catalyst, removing more material than nor-





mal. The wet filter, however, is very difficult to handle.





               Run No. 4-P was conducted to eliminate the wet first fil-





ter. During this run, the first filter remained dry and was much easier





to handle. The second filter was yellow in color after 30-min running




time. During both runs, the impinger solutions were cloudy indicating





that not all of the flue gas material was captured on the filter and




that water-soluble organics were present. Also, the filter support frit




contained condensed tar and oil. In all cases, the silica gel was dis-





colored, indicating a reaction with some substance passing through the




train or the collection of additional condensates.





               In order to most closely comply with the EPA Method 5




sampling train for particulates and organic matter, Train C (Figure 6)




was chosen for use during the actual test series. This train also had





the advantage of eliminating the wet first filter. The first filter was




to be heated to 200 to 250°F (93.3 to 121.1°C).




               Computer printouts of the field data for the preliminary




runs are presented in Appendix G.




               b.  Test series;  Particulate and organic samples were





taken with Research Appliance Company Model 2243 "Stacksampler"  equip-




ment, modified by MRI. Stack gas temperature readings were taken by
                                   28

-------
thermocouple using a Thermo Electric Minimite Model 31101 potentiometer.





Stack gas velocities were taken with the Alnor Velometer, Type 3002-2G.





               No traversing of the stacks was done due to the small





diameter of the pipes. As the stacks were made of clay sewer pipe,  the





cutting of ports was considered impractical and no extensions were  added





to the stacks in order not to disturb the natural flow characteristics.





The probe tip was merely inserted down into the center of the stack ap-




proximately 6 in. (15.3 cm). After the preliminary tests, it was believed





possible to approach an isokinetic sampling rate by working the EPA iso-





kinetic equation backwards, so to speak, for the actual gas volume  to be





sampled for each 5-min sampling period. The equation used for this  com-




putation is presented in Appendix H.





               Sampling times per stack were chosen in order to optimize




maximum time and sample volume with minimum operation and cleanup prob-





lems. Sample times per stack were as follows:




               Run No. 3                   30 min





               Run Nos. 5,7               20 min




               Run Nos. 9, 11, 13          15 min




               Run No. 14                  10 min




No direct attempt was made to hold to the general EPA guidelines of a




2-hr sample time and 60-dscf sample volume.—  Sample times were reduced




generally when the number of first filter changes became excessive  due
                                  29

-------
to filter plugging (excessive pressure drop) or when such changes were




forecast for the following run.




               Flue gas velocities were measured every 10 min for each




run until Run No. 9, when they were measured once per stack. For each




run, these velocities remained fairly constant for each stack,  within




the precision of the method of measurement. The metering console data




and flue gas temperatures were recorded every 5 min throughout  the test




series. Periodic leak checks of the train were made in order to ensure




leak-free operation. In addition, visual examination of the train was




made during sampling on nearly every stack to ensure proper functioning.




               The relationship between the run times and the burn cy-




cle has been presented in Figure 3. Run No. 1 was made in an attempt to




sample emissions during the start-up period. However, after sampling for




5 min on Stack 1, the draft became insufficient and no other stacks emit-




ted until after the doors had been closed. Therefore, Run No. 1 was com-




pleted by sampling 25 min with the probe projecting into the plume being




emitted out of the front door. A nominal duct diameter of 10 ft (3.048




m) was used in the calculations for Tables 1 through 5. Insufficient time




remained on that day to begin a normal test series.




               Standard operation was to intersperse the POM sampling




with the particulate-organic sampling. This involved using both trains




on a stack in succession before moving to the next stack. Except for the
                                   30

-------
first full day (December 3,  Run No. 3),  the POM run on a  stack  preceded





the particulate-organic run.





               The stacks were sampled in the order 1, 2,  4,  3,  5,  6,  7,





8 except during Runs Nos. 9, 11, 13,  and 14. For Run No.  9, Stacks  1 and





2 were not emitting at the start of the test so sampling  was  begun  on





Stack 4. Subsequently, Stack 1 began emitting and was sampled last. Stack





2 never emitted and was not  sampled.  On Run No. 11, Stack 2 did not begin




emitting until after the start of the test and so was sampled last. Run




No. 13 was terminated during sampling on the second stack as  a  result  of





repeated first filter changes and a difficulty in maintaining an isokine-




tic sampling rate. During Run No. 14, Stacks 4 and 8 ceased emitting and





were capped by kiln personnel, Stack 4 after being tested and Stack 8




prior to being tested. During Run No. 7,  several stacks were  emitting  in-




termittently. This "puffing" was determined by continuously monitoring




the stack temperature. No sampling was done during period of  no emissions.




               During Run No. 3, the train configuration  was  changed in





that a cyclone and catch-bottle was inserted prior to the first filter




to provide a reservoir for the collected water. Due to the high moisutre




content of the gas' stream (~ 30%), the volume of water condensed was such




that even by heating the first filter box, all of the moisture  could not




be maintained in the vapor stage. The cyclone-bottle combination was pro-




vided in order to retain this moisture and not have it fill up  the  hori-




zontal portions of the probe. During some runs, the collected water had
                                   31

-------
to be emptied to prevent overflow. This water was combined with the im-





pinger catch.





               Values for the percent moisture by volume of the gas





stream were determined in the field by measurement of the volume of wa-





ter condensate collected. Some of these values were subsequently found





to be slightly in excess of the saturation value for the average stack





temperature as read from a psycrometric chart. Therefore, the percent




moisture values for use in the computer calculations for Runs Nos.  1,  11,




13, and 14 were determined by volume calculations while those of Runs  Nos.




3, 5, 7, and 9 were determined from a psychrometric chart. The value for





Run No. 1 is very low, probably due to mixing between the atmosphere and





the plume emerging from the open kiln door.





               Two or three grab samples of the stack gas were taken per





day for ORSAT analysis of the stack gas composition. The values obtained





were averaged for each days' runs.




               No sampling was done on December 9, 1975, as all of  the




stacks were either partially or totally capped.





          2.  Polycyclic organic materials




               a.  Preliminary tests;  After the first preliminary  test




series, described earlier, the polycyclic organic material (POM) train




was modified by placing another filter in front of the sodium carbonate




impingers (Figures 7 and 8). This was done in an attempt to clean up the
                                   32

-------
              rGlass Fiber  Filter
                                                                             Glass Fiber Filter
                     T
                           8
 -350°F'    r-
             i

/-Stack      L_
                             I-—6"
2% Sodium

Carbonate
                                         Dry
                                                          Ice Bath


                                                     •Silica Gel
u>
10
                                 Figure  7 - Preliminary Sampling Train D:  Run No.  5-P
f
4
o
                              o
                             O
          »— ^

            R
                                            Glass Fiber  Filter
                        Glass Fiber Filter
                                                                   J

                                                                 Metering

                                                                 Console
                       2% Sodium

                       Carbonate
                                                                       Dry
                                                              Bath


                                                      •Silica Gel
                                  Figure 8 - Preliminary  Sampling Train E:  Run No.  6-P

-------
impinger solutions for ease of analysis. The first test  (Run No.  5-P)





was done with the first filter heated to approximately 350°F (177°C),





while the second test (Run No. 6-P) was run with both filters  at  am-




bient temperature.





               During Run No. 5-P,  the first filter remained dry. The





second filter was yellow in color after 30 min running time. Run  No.





6-P was conducted to see if condensed water would pass through a  hori-




zontal filter and frit easier than through a vertical assembly. This





proved to be the case but the wet filter was still hard  to  handle.





Again, all impinger solutions were cloudy and the filter support  frit




contained tar and oil.




               For the actual test series, Train D (Figure  7)  was chosen





in order to maintain a dry first filter and to remove as much  material




as possible prior to the impinger solutions/The first filter  was to be





heated to 200 to 250°F (93.3 to 121.1°C).




               Computer printouts of the field data for  the preliminary





runs are presented in Appendix G.




               b.  Test series;  The same sampling equipment and  tech-




niques were used for the POM testing as for the particulate-organic




testing. POM concentrations in the preliminary samples were found to be




of sufficient magnitude to allow for a minimal sampling  time during the




test series in order to keep the impinger solutions as clean as possible.
                                  34

-------
Sampling times of 5 min/stack were used for all  runs.  First  filters were





replaced as necessary.





               Flue gas velocities were measured prior to  sampling each





stack. The metering console data and flue gas temperatures were  recorded





every 5 min. Periodic leak checks and visual inspections of  the  train





were made to ensure proper functioning.





               The stacks were sampled in the same  order as  for  the




particulate-organic train with the same exceptions. For Run  No.  8, Stacks




1 and 2 were not emitting at the start of the test, Stack  1  being sampled





last and Stack 2 omitted due to lack of emissions.  On  Run  No.  10, Stack




2 did not begin emitting until midway through the test and so  was sampled




last. During Run No. 12, Run No. 13 (particulate-organic)  was  terminated.





Run No. 12 was held up until Run No. 14 had caught  up  in the number of




stacks sampled. For Run No. 12, Stack 8 was not  tested as  it was sealed




before it could be tested. During Run No. 6, several stacks  emitted only




intermittantly. This was detected by constant monitoring of  the  flue gas




temperature and no sampling was done during period  of  "puffing."




               No cyclone assembly had to be added  to  the  train  to catch




condensed water vapor but moisture collected in  the probe  elbow  prior




to the first filter was periodically added to the contents of  the first




impinger. Percent moisture values were determined as for the particulate-




organic train, those for Runs Nos. 10 and 11 calculated from volume com-




putations while those for Runs Nos. 2, 4, 6, and 8  were obtained from a




psychrometric chart.




                                  35

-------
          3.  Flammability limits and heat of combustion;   Another por-




tion of the sampling program was to determine if a flaramability limit




could be established. This is the amount of air that must  be combined




with the flue gas stream in order to sustain combustion, data useful in




exploring control device possibilities for the kilns.




          The apparatus used is shown in Figure 9. The chamber was




filled with flue gas using the inlet blower. When this was accomplished,




the inlet was directed towards ambient air and the spark or flame  source




was initiated. The flue gas in the chamber and the incoming ambient air




were mixed using the inlet and outlet blowers. Three ignition methods




were tried, two spark and one open flame.




          Several tests were attempted during the preliminary tests and




the actual test series. At no time could the flue gas be made to ignite.




It is thought that the high moisture content of the stack  gas stream may




be responsible for this failure to ignite.




          In an attempt to obtain some useful information  relating to




the combustion qualities of the stack gas, five cryogenic  samples  were




taken during the actual test series in order to determine  the heat of




combustion of the condensed material. The sampling apparatus is shown




in Figure 10. A 0.5-in. ID stainless steel "U"-tube was placed in  a dry-




ice-ethanol bach (-97.6°F, -72°C) and a sample was drawn at a very low




flow rate using the RAG meter console until the trap was sealed with
                                   36

-------
CO
                 Plexiglas
                 Front
                                        Outlet
                                        Blower
                      Spark Plug
                           Outlet
                           Blower
                                                      Inlet Blower
Inlet, Secondary
Spark Source
and Open Flame
Ports
                                                  Plywood
                                                  Chamber
                                                              Plexiglas
                                                              Front
Secondary
Spark
Source
                                        Plywood
                                        Chamber
                                a. SIDE VIEW
                   b. FRONT VIEW
                                       Figure 9 -  Flammability Limits Apparatus

-------
to
oo
                              Dewar
                              Flask
                                                    Stainless  Steel "U" -Trap
                                                             Wood
                                                             Cover
                                                           Cryogenic
                                                           Bath
Metering
Console
                                        Figure 10 - Cryogenic Sampling Apparatus

-------
condensed material. For the last two tests, a salt water-ice bath (14°F,





-10°C) was substituted for the dry ice-ethanol bath. These samples were





run for 15 min but were not cold enough to freeze.







B.  Analysis





          1.  Mass and total organicsi  At the conclusion of each run,





the samples were recovered at the sampling site. The filters were placed





in clean, wide-mouth glass jars. All filters from a given position in




the train, i.e., first or second, for each run were placed in the same




jar. All glassware ahead of the first filter was washed with acetone into





a clean, narrow-mouth glass bottle and sealed with a poly-seal cap. The





impinger water was measured volumetrically and stored in a clean, narrow-




mouth glass bottle with a poly-seal cap. The impingers, and all glassware





behind the first filter,  were then rinsed with acetone into a separate




clean, narrow-mouth glass bottle having a poly-seal cap. The silica gel





was weighed and discarded. The samples, after recovery, were transported





to Kansas City by truck for analysis.




          For the first set of preliminary runs, it was believed that




the sodium carbonate solution could be utilized for both mass-organic




and POM evaluations. However,  it was discovered that the sodium carbon-




ate was taken up by the ether-chloroform extraction process,  resulting




in a white,  crystalline mass in the sample residue. Thus, the train con-




figuration was changed for the other preliminary series and for the actual




test series.
                                  39

-------
          The mass samples were analyzed as specified in the referenced




Federal Register«~  To obtain data for the total organics portion of the




task, the filters were extracted ultrasonically using three 25-ml por-




tions of chloroform followed by three 25-ml portions of ether. Each por-




tion was decanted from the filter residue using disposable pipettes. The




filter particles collected in the ether-chloroform extract were then cen-




trifuged out and rinsed with ether and chloroform until no color was de-




tected in the rinses. The combined ether-chloroform washings were evapor-




ated in an ambient air hood, dessicated, and weighed. This result was




compared with that of the total mass filter weight and the organic frac-




tion was determined. This fraction was then applied to the acetone rinses




to determine their organic fractions. The total organic load was obtained




by summing all of the organic fractions with the result of the ether-




chloroform extraction of the impinger water.




          2.  Polycyclic organic materials;  The POM samples were re-




covered in the field in the same manner as the mass samples except that




clean, brown-glass bottles with poly-seal caps were used for all solu-




tions.




          The sodium carbonate impinger solutions were extracted in a




separatory funnel using three 100-ml portions of cyclohexane. The acetone




rinses were evaporated to dryness using a stream of nitrogen gas. They




were then extracted with cyclohexane, using 20-, 20-, and 5-ml portions.
                                   40

-------
The filters were extracted ultrasonically using cyclohexane,  also using




20-, 20-, and 5-ml portions. The extractions were eluted on 20-gram col-




umns of fluorisil eluted with 250 ml of 15% ether in hexane.  The samples




were analyzed using a Varian Model 1400 gas chromatograph with a scandium




tritide electron capture detector. The 6 ft by 2 mm ID glass  column was




packed with 3% Dexil 300 GC on 100/120 Supelcoport. A nitrogen carrier




gas flow rate of 30 ml/min was used. The temperatures utilized for the




injection port, column, and detector were 255, 290 and 295°C,  respectively.




          3.  Heat of combustion;  The cryogenic samples were recovered




after the return to Kansas City. The stainless steel U-traps  were opened




and the water fraction of each trap poured into a separate clean glass




bottle and sealed with a poly-seal cap. The material remaining in each




trap was then rinsed with acetone into separate clean glass bottles. The




acetone rinses were evaporated to dryness at approximately 55°C,  cooled




to room temperature, and sealed with poly-seal caps. Both sets of samples




were weighed and then sent to Kansas City Testing Laboratories for anal-




ysis. The heat of combustion results were obtained by Adiabatic Bomb




Calorimeter. Filter paper pellets were used as a fuel source  for both




the water and the tar and oil fractions. The tar and oil fraction samples




were transferred to the bomb cup via filter paper. A slight residue was




observed in the bomb cup after each firing, indicating that the values




may be on the low side.
                                  41

-------
                   V.  RECOMMENDATIONS AND COMMENTS







          !•  The data presented in this report results from a single





series of tests at a single kiln. It is not known how various woods  would





effect the emission characteristics. Other factors that could play a role





are the meterological conditions and kiln operator techniques. Prior to





any extensive setting of regulations regarding the charcoal  kiln  industry,





other tests at other kilns should be considered to evaluate  these other




factors.





          2.  It is possible that more uniform mass data could be obtained




by sampling with a train that does not employ the first filter, similar





to the EPA sampling train for sulfuric acid mist.—  In this  train, the




flue gas stream is passed directly to the impingers before going  to  a





final filter. This would eliminate the constant need for replacement of




the first filter resulting from heavy loading and excessive  pressure





drop across the filter. Also, due to the nature of the flue  gas stream,




the amount of material that passes through the filter is somewhat depen-




dent on the temperature at which the first filter is maintained in the




sample box. Because of the variations in the precision of different  sam-




ple box heaters, the amount of material collected on the first filter




could vary from test to test, thus affecting the "front-half" emission





calculations. By going to the impingers directly, the need to heat the




probe or otherwise handle the condensed flue gas water vapor would be




eliminated.







                                  42

-------
          3.  The low stack gas velocity inherent in charcoal  kiln op-




eration is difficult to measure by normal means•  The velometer used in




this test worked satisfactorily but as has been mentioned,  is  affected




by ambient wind and possibly by the flue gas constituents.  Other methods




should be investigated to determine the most suitable.




          4.  Further work needs to be done to determine the combustion




characteristics of the flue gas stream if control methods are  envisioned




for the charcoal industry. Enhanced combustion might be achieved by re-




moving all or part of the water vapor from the flue gas stream. The pos-




sibility of using charcoal as the heat source for waste gas combustion




might also be explored.
                                  43

-------
                              REFERENCES
1.  Environmental Protection Agency,  "Standards of Performance for New
      Stationary Sources," Federal  Register, Vol. 36, No. 159, Part II,
      Tuesday, August 17,  1971.

2.  Engineering Science, Inc.,  "Exhaust Gases  from Combustion and Indus-
      trial Processes," Chapter  IV-3, Environmental Protection Agency
      Contract No. EHSD 71-36, October 1971.

3.  Jarvis, J. Pitts, Jr., "The  Wood  Charcoal  Industry in the State of
      Missouri," Engineering Series Bulletin No. 48, Engineering Exper-
      iment Station,  University  of  Missouri at Columbia, Vol. 61, No.
      21, Columbia, Missouri, May 2,  1960.

4.  Sverdrup & Parcel and  Associates, Inc., "Air Pollution Control for
      Missouri Charcoal Kilns,"  prepared  for the Missouri Air Conserva-
      tion Commission, Jefferson City, Missouri, February 1971.

5.  Hodgman, Charles  D. (ed.), Handbook of Chemistry and Physics, 23rd
      Ed., Chemical Rubber Publishing Company, Cleveland, Ohio (1939).

6.  Dean, John A. (ed.), Lange's Handbook of Chemistry, llth Ed., McGraw-
      Hill Book Company, New York (1973).
                                  44

-------
                APPENDIX A
RESULTS OF ANALYSIS - COMPUTER COMPUTATIONS
            (TOTAL PARTICULATE)
                     45

-------
                  TABLE A-l




PARTICULATE DATA  AND  CALCULATED VALUES
RUN- 1
ATMOS
TEMP
(06. F)
60.0
PORT-
POINT

1
D
I)
0
D
f)
ATMOS
PHES
(I.HG)
29.26
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
802.84
804.15
806.04
808.02
810.29
812.96
H?0
COND
(ML)
31.0
DELTA
P
I.H20)
.002
.008
.008
.008
.008
.008
PARTIC
WT-PTL
(MG)
786.70
DELTA
II
(I.H20)
.150
.250
.400
.450
.550
.850
OATH- 12-02-75
PARTIC STACK
WT-TTL
(MG)
955
TEMP
IN
(D.F)
62.0
64.0
67.0
72.0
80.0
85.0
.70
TEMP
OUT
(D.F)
62.0
64.0
64.0
64.0
6Q.O
69.0
AREA
(FT?)

TRAIN
VAC
(I.HG)
1.0
1.0
2.0
2.5
4.0
5.5
INIT
VOL
(DCF)
801.61
STACK
TEMP
(D.F)
62.0
50.0
50.0
50.0
50.0
50.0
PERC PERC PERC PI
02 C02
DRY DRY
9.2 11.0
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
.600
.600
CO T
TOT
URF
DRY COFF
1.9 .

VP.L
(FPH
150.
300.
300.
300.
300.
300.
050


)
0
0
0
0
0
0

-------
                  TABLE A-2
PARTICULATE DATA  AND  CALCULATED VALUES
ATMOS
TEMP
(DG
40
.F )
.0
PORT-
PO

1
1
1
1
1
1
2
2
2
2
2
2
4
4
4
4
4
4
INT

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
ATMOS
PRES
( I . HG )
29.31
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
RUN- 3
H?0 PARTIC
COND WT-PTL
(I.H20) (ML)
0.00
METER
VOL
(DCF) 1
814.74
816.47
818.17
819.87
821.61
823.47
825.05
826.78
828.66
830.53
832.47
834.18
836.32
838.47
840.49
842.42
844.38
846.64
675.2
DELTA
P
(I.H20)
.006
.006
.006
.006
.006
.006
.006
.006
.006
.006
.006
.006
.009
.009
.007
.007
.009
.009
(MG)
2162.50
DELTA
H
U.H?0)
.400
.350
.330
.350
.370
.400
.300
.400
.440
.400
.350
.350
.550
.530
.450
.400
.500
.550
DATE- 12-03-75
PARTIC STACK INIT
WT-TTL AREA VOL
(MG) (FT?)
4855
TEMP
IN
(D.F)
42.0
46.0
56.0
59.0
66.0
69.0
56.0
61.0
72.0
64.0
72.0
74.0
65.0
71.0
79.0
80.0
85.0
87.0
.10
TEMP
OUT
(D.F)
44.0
44.0
44.0
45.0
48.0
49.0
55.0
56.0
58.0
59.0
60.0
61.0
62.0
63.0
64.0
65.0
66.0
68.0
.20
TRAIN
VAC
(I.HG)
2.5
2.5
3.0
4.0
7.0
7.5
11.0
14.0
14.0
4.0
9.0
9.0
10.0
6.5
6.5
6.5
8.0
9.0
(DCF)
813.01
STACK
TEMP
(D.F)
145.0
140.0
140.0
140.0
140.0
140.0
150.0
150.0
150,0
145.0
150.0
150.0
130.0
130.0
135.0
135.0
130.0
135.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY DRY COEF
9.2 11.0 1
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
50.0 .600
.600
50.0 .600
.600
50.0 .600
.600
.600
.600
.600
.600
.600
.600
.600
.600
50.0 .600
.600
.9 .850

VEL
(FI'M)
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
350.0
350.0
320.0
320.0
350.0
350.0

-------
                                            TABLE A-2  (Concluded)
                                     RUN-
DATE-  12-03-75
00
PORT-
PO

3
3
3
3
3
3
5
5
5
5
5
5
6
6
6
6
6
6
7
7
7
7
7
7
8
8
8
8
8
8
INT

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(M1N)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF)
848.58
850.39
852.26
854.17
656.33
858.82
860.99
863.59
066.03
868.03
870.31
872.79
875.34
878.03
880.37
882.08
884.03
886.24
888.17
889.99
891.61
893.37
894.87
896.38
898.77
901.12
903.36
905.49
907.40
909.35
HELTA
P
(I.H20)
.006
.006
.008
.008
.009
.009
.011
.011
.008
.008
.014
.014
.011
.011
.006
.006
.008
.008
.006
.006
.005
.005
.004
.004
.011
.011
.008
.008
.007
.007
DELTA
H
(I.H20)
.500
.400
.450
.400
.500
.700
.700
.750
.700
.600
.750
.700
.750
.800
.800
.550
.550
.650
.550
.450
.400
.400
.300
.300
.650
.650
.550
.550
.400
.400
TEMP
IN
(D.F)
65.0
70.0
80.0
83.0
81.0
87.0
76.0
82.0
95.0
94.0
98.0
100.0
82.0
«9.0
98.0
98.0
98.0
100.0
86.0
90.0
95.0
97.0
100.0
98.0
82.0
87.0
95.0
96.0
99.0
99.0
TEMP
OUT
(D.F)
66.0
66.0
67.0
68.0
70.0
72.0
73.0
74.0
75.0
76.0
77.0
78.0
78.0
79.0
80.0
80.0
81.0
82.0
82.0
82.0
82.0
83.0
84.0
84.0
81.0
82.0
82.0
82.0
82.0
82.0
TRAIN
VAC
(I.HG)
11.0
11.0
14.0
15.0
6.0
6.0
6.0
7.5
7.5
8.0
10.0
14.0
6.0
7.0
7.0
7.0
8.0
10.0
8.0
n.O
10.0
11.0
12.0
13.0
6.0
6.5
7.0
7.0
7.0
7.0
STACK
TEMP
(D.F)
145.0
145.0
145.0
145.0
140.0
140.0
160.0
165.0
160.0
160.0
165.0
165.0
160.0
160.0
160.0
160.0
160.0
160.0
155.0
150.0
155.0
155.0
155.0
155.0
165.0
165.0
160.0
160.0
160.0
160.0
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
50.0 .600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
70.0 .600
.600
.600
.600
60.0 .600
.600
.600
.600
.600
.600
.600
.600
55.0 .600
.600

VEL
(FPM)
300.0
300.0
350.0
350.0
350.0
350.0
400.0
400.0
350.0
350.0
450.0
450.0
400.0
400.0
300.0
300.0
350.0
350.0
300.0
300.0
280.0
200.0
250.0
250.0
400.0
400.0
350.0
350.0
320.0
320.0

-------
                 TABLE A-3
PARTICIPATE DATA AMD CALCULATED VALUES
ATMOS
TEMP
U)G
50
.F)
.0
PORT-
PO

1
1
1
1
2
2
2
2
4
4
4
4
3
3
3
3
INT

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
ATMOS
PRES

-------
t_n
O
                                                TABLE A-3   (Concluded)


                                           IU)M-    5        DATE- 12-04-75
PORT-
PO

5
5
5
5
6
6
6
6
7
7
7
7
B
8
8
B
INT

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
942.89
945.26
947.63
950.01
952.39
954.77
957.19
959.60
961.40
963.18
964.95
966.73
969.13
971.54
973.93
976.43
DELTA
P
I.H?0)
.011
• Oil
.01 1
.01 1
.011
.011
.011
.011
.006
.006
.006
.006
.011
.011
.011
.011
DELTA
H
(I.H20)
.700
.700
.650
.650
.700
.650
.700
.700
.500
.400
.350
.300
.650
.650
.650
.650
TEMP
IN
(O.F)
73.0
79.0
91.0
95.0
83,0
90.0
100.0
103.0
86.0
89.0
95.0
97.0
90.0
96.0
104.0
108.0
TEMP
OUT
(D.F)
65.0
75.0
76.0
77.0
80.0
81.0
83. 0
83.0
84.0
05.0
86.0
87.0
86.0
88.0
88.0
90.0
TRAIN
VAC
(I.HG)
6.0
7.5
9.0
9.0
10.0
11.0
11.5
12.0
5.0
5.0
5.5
6.5
10.0
10.5
11.5
12.0
STACK
TEMP
(D.F)
160.0
155.0
160.0
160.0
160.0
160.0
165.0
160.0
165.0
165.0
165.0
165.0
165.0
165.0
160.0
160.0
S.GEL PROBE
TEMP T niA
(D.F) (IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
65.0 .600
.600
.600
.600
.600
.600

VEl.
(FPM)
400.0
400.0
400.0
400.0
400.0
400.0
AOO.O
400.0
300.0
300.0
300.0
300.0
400.0
400.0
400.0
400.0

-------
                  TABLE A-4
PARTICULATE  DATA  AND CALCULATED  VALUES
ATMOS
TEMP
(06.
50.
F)
0
PORT-
POINT

1
1
1
1
2
2
2
2
4
4
4
4
3
3
3
3

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
ATMOS
PRES
(I.HG)
29.25
SAMP
TIME
( 1-1 1 N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) <
978.81
980.18
981.61
983.08
984.80
986.52
988.47
990.56
992.31
994.20
995.95
997.72
999.19
1000.66
1002.10
1003.49
RUN- 7
H?0 PARTIC
COND WT-PTL
(ML)
624.7
DELTA
P
I.H20)
.004
.004
.004
.004
.006
.006
.008
.008
.006
.006
.006
.006
.004
.004
.004
.004
(MG)
10536.20
DELTA
H
(I.H20)
.300
.250
.250
.250
.350
.300
.400
.500
.350
.450
.400
.400
.300
.250
.250
.250
DATE.- 12-05-75
PARTIC STACK
WT-TTL AREA
(MG) 1
62150
TEMP
IN
(O.F)
64.0
68.0
72.0
74.0
72.0
77.0
85.0
88.0
78.0
81.0
90.0
92.0
80.0
82.0
88.0
90.0
.60
TEMP
OUT
(D.F)
66.0
67.0
67.0
68. 0
70.0
71.0
73.0
74.0
76.0
77.0
78.0
79.0
80.0
80.0
81.0
82.0
!FT2)
.20
TRAIN
VAC
(I.HG)
4.0
4.0
4.0
4.0
5.0
6.0
8.0
8.5
10.0
11.0
1?.0
12.0
4.0
5.0
5.0
6.0
INIT
VOL
(DCF)
977.30
STACK
TEMP
(D.F)
155.0
155.0
150.0
150.0
155.0
150.0
150.0
150.0
165.0
160.0
165.0
160.0
160.0
160.0
160.0
160.0
PERC PERC PERC PITOT
02 C02 CO TUBF
DRY DRY DRY COEF
9.2 17.2 4
S.GEL PROBE
TEMP T DIA
(O.F) (IN)
.600
.600
60.0 .600
.600
.600
.600
65.0 .600
.600
.600
.600
.600
.600
.600
.600
60.0 .600
.600
.1 .850

VEL
(FPM)
250.0
250.0
250.0
250.0
300.0
300.0
350.0
350.0
300.0
300.0
300.0
300.0
250.0
250.0
250.0
250.0

-------
                                               TABLE A-4  (Concluded)
                                        RUM-
DATE- 12-05-75
Ol
N>
PORT-
PO

5
5
5
5
6
6
6
6
7
7
7
7
8
8
8
H
INT

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF)
1005.43
1007.39
1009.53
1011.61
1013.61
1015.64
1017.64
1019.41
1021.70
1023.97
1026.25
102B.50
1029.96
1031.42
1032.96
1034.54
DELTA
P
(I.H20)
.008
.008
.008
.000
.008
.008
.007
.007
.010
.010
.010
.010
.004
.004
.005
.005
DELTA TEMP
H
(I.H20)
.450
.450
.550
.550
.550
.500
.450
.350
.700
.700
.650
.650
.400
.400
.300
.300
IN
(D.F)
70.0
74.0
84.0
87.0
77.0
83.0
92.0
94.0
84.0
92.0
98.0
103.0
80.0
81.0
86.0
89.0
TEMP
OUT
(D.F)
74.0
74.0
74.0
75.0
77.0
78.0
79.0
80.0
80.0
82.0
83.0
84.0
80.0
ei.o
82.0
81.0
TRAIN
VAC
(I.HG)
9.0
10.0
11.0
11.0
5.0
9.0
10.0
9.0
12.0
12.0
12.0
12.5
5.0
9.0
9.0
9.0
STACK
TEMP
(D.F)
160.0
165.0
165.0
170.0
170.0
165.0
160.0
165.0
185.0
185.0
190.0
185.0
180.0
175.0
175.0
175.0
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600

VEL
(FPM)
350.0
350.0
350.0
350.0
350.0
350.0
325.0
325.0
400.0
400.0
400.0
400.0
250.0
250.0
275.0
275.0

-------
                                               TABLE A-5
                              PART1CULATE DATA  AND  CALCULATED VALUES
Ul
OJ
ATMOS
TEMP
(DG.F)
40.0
PORT-
POINT

4 1
4 1
4 1
3 1
3 1
3 1
5 1
5 1
5 1
6 1
6 1
6 1
ATMOS
PRES
(I.HG)
29. 6b
SAMP
TIME
( M I M )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(1.H20)
0.00
METER
VOL
(OCF) (
36.12
37.68
39.44
41.1?
42.73
44.51
46.19
47.87
49.55
50.96
52.36
53.76
HUN- 9
H20 PARTIC
COND
(ML)
316.4
DELTA
P
I.H20)
.006
.006
.006
.006
.006
.006
.006
.006
.006
.004
.004
.004
WT-PTL
(MG)
3719.50
DELTA
H
(I.H20)
.300
.350
.400
.400
.400
.400
.400
.400
.350
.250
.250
.250
DATE- 1
PARTIC
WT-TTL
(MG)
8569
TEMP
IN
(D.F)
40.0
43.0
49.0
48.0
51.0
57.0
51.0
55.0
60.0
54.0
58. 0
60.0
.10
TEMP
OUT
(D.F)
40.0
41.0
42.0
45.0
46.0
47.0
50.0
50.0
51.0
52.0
52.0
53.0
2-06-75
STACK
AREA
(FT2)
.20
TRAIN
VAC
(I.HG)
4.0
5.0
6.5
fl.O
8.0
9.0
9.0
9.5
10.0
10.0
10.5
11.0
INIT
VOL
(DCF)
34.54
STACK
TEMP
(D.F)
155.0
160.0
160.0
145.0
145.0
145.0
150.0
155.0
155.0
150.0
155.0
155.0
PF.RC PERC PERC PI
02 C02
DRY DRY
6.4 16.1
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
TOT
CO TURF.
DRY COEF
1.5 .

VFL
(FPM
300.
300.
300.
300.
300.
300.
300.
300.
300.
250.
250.
250.
850


)
0
0
0
0
0
0
0
0
0
0
0
0

-------
Ln
-P-
                                            TABLE A-5  (Concluded)

                                      »«UN-     9      OATE-  12-06-75
PORT-
POINT

7
7
7
8
8
8
1
1
1

1
I
I
1
1
i
i
i
i
SAMP
TIME
(HIM)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
55.53
57.10
58.69
60.44
63.05
63.70
65.39
67.09
68.72
DELTA
P
I.H20) 1
.006
.006
.006
.006
.006
.006
.006
.006
.006
DELTA
H
II.H20)
.400
.350
.300
.400
.350
.350
.350
.350
.350
TEMP
IN
(D.F)
55.0
59.0
63.0
54.0
58.0
63.0
60.0
64.0
68.0
TEMP
OUT
(D.F)
54.0
55.0
55.0
55.0
56.0
56.0
56.0
56.0
58.0
TRAIN
VAC
STACK S.GEL PROBE
TEMP TEMP T 01 A
(I.HG) ('D.F) (D.
4.0
5.0
7.5
13.0
13.0
12.0
11.0
12.5
13.0
165.0
165.0
165.0
165.0
170.0
170.0
155.0
155.0
160.0
,F) (IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
VFL
(FPM)
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0

-------
                  TABLE A-6
PARTICIPATE DATA  AND CALCULATED VALUES
ATMOS
TEMP
(DO
40
.F)
.0
PORT-
PO

1
1
1
4
4
4
3
3
3
5
5
5
6
6
6
INT

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
ATMOS
PRES
(I.HG)
29.65
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
CDCF) (
72.13
73.50
74.86
76.66
78.44
80.25
81.87
B3.43
84.83
86.49
88.34
90.09
91.69
93.32
94.94
RUN- 1 1
H20 PAPTIC
COND WT-PTL
(ML)
370.0
DELTA
P
I.H20)
.004
.004
.004
.008
.008
.000
.006
.006
.006
.006
.006
.006
.006
.006
.006
(MG)
6043.60
DELTA
H
(I.H20)
.250
.250
.250
.400
.400
.400
.300
.300
.300
.350
.400
.400
.400
.350
.350
OATE- 12-07-75
PARTIC STACK ]
WT-TTL AREA
(MG) 1
12969
TEMP
IN
(D.F)
44.0
47.0
51.0
48.0
53.0
59.0
52.0
5M.O
62.0
52.0
57.0
63.0
55.0
59.0
65.0
.50
TEMP
OUT
(D.F)
45.0
45.0
45.0
46.0
47.0
47.0
48.0
49.0
50.0
50.0
51.0
51.0
52.0
53.0
54.0
IFT2)
.20
TRAIN
VAC
(I.HG)
3.0
4.0
6.0
9.0
9.0
9.5
9.5
11.0
13.5
3.0
3.0
4.0
4.0
4.0
5.0
[NIT
VOL
(DCF)
70.83
STACK
TEMP
(D.F)
170.0
170.0
170.0
200.0
200.0
205.0
170.0
160.0
160.0
170.0
185.0
190.0
175.0
180.0
100.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY DRY COF.F
5.1 18.2 5.
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
.600
56.0 .600
.600
.600
.600
.600
50.0 .600
.600
.600
.600
.600
5 .850

VEL
(FPM)
250.0
250.0
250.0
350.0
350.0
350.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0

-------
                                            TABLE A-6  (Concluded)
                                       RUN-   11
DATE-  12-07-75
Ln
PORT-
POINT

7
7
7
8
8
8
2
2
?.

1
1
1
1
I
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF )
96.57
9B.16
99.72
101.28
102.85
104.42
105.74
107.04
108.36
DELTA
P
(I.H20)
.006
.006
.006
.006
.006
.006
.005
.005
.005
DELTA
H
(I.H20)
.350
.350
.300
.300
.300
.300
.250
.200
.200
TEMP
IN
(D.F)
53.0
57.0
61.0
59.0
62.0
65.0
60.0
62.0
66.0
TEMP
OUT
(D.F)
54.0
55.0
55.0
55.0
56.0
57.0
58.0
58.0
58.0
TRAIN
VAC
(I.HG)
5.0
6.0
6.0
7.0
8.0
8.0
7.0
7.0
8.0
STACK
TEMP
(D.F)
1H5.0
195.0
190.0
205.0
205.0
205.0
335.0
330.0
330.0
S.GEL PROBE
TEMP T 01 A
(D.F) (IN)
.600
55.0 .600
.600
.600
.600
.600
.600
50.0 .600
.600

VEL
(FPM)
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0

-------
                 TABLE A-7



PARTICULATE DATA AND CALCULATED  VALUES
RUN- 13
ATMOS
TEMP
(DG.F)
40.0
PORT-
POINT
1 1
1 1
1 1
2 1
2 1
ATMOS
PRES
(I.HG)
29.35
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(OCF) (
112.45
113.52
115.01
116.04
116.76
M?0
COND
(ML)
52.5
DELTA
P
I.H20)
.005
.005
.005
.003
.003
PARTIC
WT-PTL
(MG)
1577. ao
DELTA
H
(I.H20)
.250
.200
.300
.100
.050
DATE- 12-08-75
PARTIC STACK
WT-TTL AREA
(MG) (FT2)
2566.
TEMP
IN
(D.F) (
42.0
45.0
50.0
42.0
45.0
30
TEMP
OUT
D.F)
45.0
45.0
45.0
44.0
45.0
.20
TRAIN
VAC
(I.HG)
9.0
14.0
5.0
10.0
15.0
INIT
VOL
(DCF)
111.14
STACK
TEMP
(D.F)
320.0
325.0
290.0
320.0
330.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY DRY COEF
1.1 22.3 6.
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
.600
7 .850
VEL
(FPM)
300.0
300.0
300.0
250.0
250.0

-------
                                               TABLE A-8




                              PARTICIPATE  DATA AND CALCULATED  VALUES
oo
ATMOS
TEMP
( 06 . F
40.0
PORT

)


POINT

1
1
2
2
4
4
3
3
5
5
6
6
7
7

1
1
1
1
1
1
1
1
1
1
1
1
1
1
ATMOS
PRES
(I.HG)
39.35
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(1.H20)
0.00
METER
VOL
(DCF) (
118.09
119.36
120.31
120.98
122.15
123.22
124.27
125.27
126.59
127.71
129.27
130.65
132.00
133.17
RUM- 14
H?0 PARTIC
COND
(ML)
176.0
DELTA
P
I.H20)
.005
.005
.002
.002
.003
.003
.003
.002
.006
.006
.004
.004
.004
.004
WT-PTL
(MG)
6858.70
DELTA
H
(I.H20)
.200
.200
.100
.100
.200
.200
.200
.150
.250
.150
.300
.300
.300
.250
DATE- 1
PARTIC
WT-TTL
(MG)
10048
TEMP
IN
(D.F)
43.0
46.0
46.0
47.0
50.0
53.0
45.0
47.0
46.0
48.0
49.0
54.0
52.0
55.0
.90
TEMP
OUT
(D.F)
45.0
46.0
46.0
47.0
4«.0
4 8 . 0
47.0
47.0
47.0
47.0
47.0
48.0
49.0
50.0
2-08-75
STACK INIT
AREA
(FT2)
.20
TRAIN
VAC
(I.HG)
2.5
5.0
7.0
12.0
4.0
10.0
4.0
11.0
8.0
e.o
4.0
9.0
1.0
2.0
VOL
(DCF)
116.76
STACK
TEMP
(O.F)
325.0
320.0
325.0
330.0
235.0
245.0
200.0
215.0
335.0
335.0
295.0
325.0
300.0
325.0
PERC PERC PERC PITOT
02 C02
DRY DRY
l.l 22.3
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
50.0 .600
.600
.600
.ISOO
.600
50.0 .600
.600
.600
.600
50.0 .600
.600
.600
.600
.600
CO TUBE
DRY COEF
6.7 .850

Vfc-L
(FPM)
300.0
300.0
200.0
200.0
220.0
220.0
200.0
200.0
340.0
340.0
200.0
280.0
280.0
280.0

-------
                                  TABLE A-9

                         PARTICIPATE EMISSION DATA
NAME       DESCRIPTION
        DATE OF RUN
UNITS      1
         12-02-75   12-03-75   12-04-75
DN
TT
PB
PM
VM
TM
VMSTD
V*'
vwv
PMOS
MD
PC02
P02
PCO
PN2
MWD
MW
CP
DPS .
TS
NP
PST
PS
vs
.AS 	 	
QS
QA
PERI
MF
MT
1C .
CAN
CAO
CAT
CAU
CAW
CAX...
EA
PROBE TIP ..DIAME.IER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP.
VOL DRY GAS-METER COND
AVG GAS METER TEMP
... VOL DRY..GAS-S.TD .COND 	
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE. BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL, DRY
PERCENT.. 0.2 .t.Y...VOL.»_..DRY ... ._
PERCENT CO 3Y VOL, DRY
PERCENT N2 BY VOL, DRY
MOLECULAR-.-*! -.DR.Y.. .STK GAS
MOLECULAR *'T-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC. .PRES .OF STACK.
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
STACK. A«EA 	 	 . .
STK FLOwRATE, DRYtSTD CN
ACTUAL STACK FLOfcRATE
PERCENT ISOKINEJIC 	
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC...IHPJMGER_CA1CH 	
PART. LOAD-PTL,STD CN
PART. LOAD-TTL,STD CN
..PART.. LQAD-PILjSTK.CN..
PART. LOAO-TTL,STK CM
PARTIC EMIS-PARTIAL
P A RT I C. . E M I S.-T.OJ Al 	
PERCENT EXCESS AIR
	 - IN _..
MIN
IN.HG
IN.H20
OCF
DEG.F
	 DSCF 	
ML
SCF









1N.K20
OEP.F

.. IN . HG
IN.HG
FPM
	 IN2. ...
DSCFM
ACFM

MG
MG
	 	
GR/DSCF
GR/DSCF
GR/ACF
GR/ACF
L8/HR
	 LB/.KS. 	

.600
30.0
29.26
.442
11.35
68.4
- Jl»15.
31.0
1.47
11.6
.884
11.0
9.2
1.9
77.9
30.13.
28.72
.850
.007
52.0
6
-0.00
29.26
275 ,
11, 310='.
a 1
19,326='
21,601-
76.7
786.70
955.70
. 17.68
1.08703
1.32054
.97224
1.18110
180
219
67
,600
240.0
29.31
..506
96.34
75.5
93.53
675.2
32.00
25.5
.745
11.0
.9.2
1.9
77.9
30.13
27.04
.650
.008
150.5
46
-0.00
29.31
332
29
42
66
94. C.
2162.50
4855.10
	 55.46.
.35606
.79940
•Z256Q
.50651
.13k/
	 .29-k/..
67
.600
160.0
29.31
.539
67. OB
79. B
64.61
596.0
26.35
30.5
.695
15.0
7.3
2.9
74.8
30.69
26.82
.850
.006
15S.3
3?
-0.00
29.31
353
29
1 1
71
99.5
3178.70
9264.70
65.69
.75769
2.20837
.44224
1.28895 .
.27k/
.78k/
4?
 £/  Nominal 10-ft (120 in.) diameter stack.
 b/  Per stack; to obtain total for kiln, multiply by 8.
                                    59

-------
                            TABLE A-9  (Continued)
                         PARTICIPATE EMISSION DATA
NAME       DESCRIPTION
        DATE OF RUN
UNITS
11
         12-05-75   12-06-75   12-07-75
DN
TT
PB
PM .. ..
VM
TM
VMSTD
VW
VWV
PMOS
MD
PC02
P02
PCO
PN2
MWD
MW
CP
DPS
TS
NP
PST
PS
VS
AS
OS
OA
PEP- 1
MF
MT
1C
CAN
CAO
CAT .
CAU
CAW
CAX
EA
.PROBE.. TIP ILI.AM.ET.ER. 	
NET TIMt OF RUN
BAROMETRIC PRESSURE
A.V.G. .ORIFICE PRES .DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL .DKY._.GAS-STD....COND 	
TOTAL M20 COLLECTED
VOL H20 VAPOR-STD COND
.PERCENT MQIST.UPE.JBY. VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL» DRY
PERCENT 0?_.6Y...V.O.Lf. DPY. _.
PERCENT CO BY VOL, DRY
PERCENT N2 BY VOL» DRY
MOLECULAR .wT-DRY ..STK_..GA.S
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD ..
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF. .STACK..
STACK PRESSURE* ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE* DRY.STD CN
ACTUAL STACK FLOwRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAU-PTL*STD CN
PART. LOAD-TTL»STD CN
PART. LOApj-PTL.»STK ..CN . . .
PART. LOAD-TTL»STK CN
PARTIC EMIS-PARTIAL
P A R T I C. EMI S- T_Q T AJ 	
PERCENT EXCESS AIR
	 	 IN..
WIN
IN.HG
IN.HZO .
DCF
DEG.F
D.SCF.
ML
' SCF









IN.HZO
DEG.F

...IN.HG
IN.HG
FPM
IN2.
DSCrM
ACFK

MG"
MG

GR/DSCF
GR/DSCF
GP/ACF
GR/ACF
LB/HR
.. .LB/.HP..

..600--
160.0
29.25
. . .. .412
57.24
79.6
- 55.00
6?4.7
29.61
35.0
.650
17.2
	 .9.2
4.1
6S.5
31.12
26.53
.850
.006
16^.8
32
-0.00
29.25
309
.29
33
62
1.04.6
10536.20
62150.60
.. .83.05
2.95024
17.40280
1.59022
9.38035,
.84i/
4.98£/.
64
...600-
105.0
29.65
.35G
34.18
53.3
35.00.
316.4
15.00
30.0
.700
lf>. 1
. 6.4.
1.5
76.0
30.63
26.98
.850
,.006 ..
157.1
21
-0.00
29.65
293
. 29
35
59
97. .0
3719.50
6569.10
56.59
1.63650
3.77023
.97498
2.24620
.49k/
.. -i.iak/.
39
.6.00
120.0
29.65
.319
37.53
54.4
-3?,. 35
370.0
17.54
31.4
.686
18.2
. 5.1
5.5
71.?
.31.12
27.00
.850
.006
202.7
24
-0.00
29.65
300
29
33
60
99.4
6043.60
12969.50
53.40
2.42671
5.20770
1.31975
2.83217
.68*'
.. . 1.461/
14
    aj  Per stack; to obtain total  for kiln, multiply by 8.
    b/  Per stackj to obtain total  for kiln, multiply by 7.
                                    60

-------
                        TABLE A-9  (Concluded)

                           PARTICULATE EMISSION DATA
 NAME
DESCRIPTION
UNITS
13

ON
TT
PB
PK
VM
TM
VMSTD
VW
VWV
PMOS
MO
PC02
P02
PCO
PN2
MWD
MW
CP
DPS
TS
NP
PST
PS
vs
AS
QS
QA
PERI
MF
MT
1C
CAN
CAO
CAT
CAU
CAW
CAX
EA
DATE OF RUN
PROBE TIP DIAMETER 	
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP ...
VOL DRY GAS-METER CONO
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL.
MOLE FRACTION DRY GAS
PERCENT C02 BY VOLt DRY
PERCENT 02 BY VOL» DRY
PERCENT CO BY VOL» DRY
PERCENT N2 BY VOL» DRY
MOLECULAR WT-DR.Y STK....6AS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD ..
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE, DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAD-PTU5TD CN
PART. LOAO-TTL»STD CN
PART. LOAp-PTLirSTK^CN 	
PART. LOAD-TTL»STK CN
PARTIC EMIS-PARTIAL
PARTIC EMIS-TOTAL
PERCENT EXCESS AIR

	 IN.
MIN
IN.HG
.IN.H20 . .
DCF
DEG.F
DSCF
ML
SCF









IN.H20
DEG.F

IN.HG
IN.HG
FPM
IN 2 ....
DSCFM
ACFM

MG
MG

GR/DSCF
GR/DSCF
GR/ACF
GR/ACF
L8/HR
LB/HR

12-08-75
. ...^600
25.0
29.35
	 _.180
5.62
44.8
... 5.79
52.5
2.49
.. .30.1
.699
22.3
.1.1..
6.7
69.9
	 31.61...
27.52
.850
.. .004
317.0
5
_ ....TO..OCL.
29.35
280
	 	 29.
26
56
J99.7..
1577.80
2566.30
38,52
4,19602
6,82485
1.96373
3.19402
.94£/
1.531/
-11
12-08-75
.600
70.0
29.35
. - .207
16.41
46.0
16.80
176.0
3.34
33.2
.666
22.3
1.1
6.7
69.9
. 31.61
27.10
.850
.004
293.6
14
-0.00
29.35
260
29
24
52
101,7
6858.70
10048.90
31.75
6.28550
9.20908
2,89786
4.24575
1.29k/
1.89k/
-11
aj  Per  stackj to obtain total multiply by 1.67
b/  Per  stack; to obtain total  for kiln, multiply by 7.
                                  61

-------
                                 TABLE A-10
                         PARTICIPATE EMISSION  DATA
                                (METRIC RE SULTS)
NAME       DESCRIPTION


        DATE OF RUN
UNITS      1           3          5

         12-02-75   12-03-75   12-04-75
ON
TT
PB
PM
VM
TM
VMSTM
VW
VWM
PMOS
MD
PC02
P02
PCO
PN2
MWD
MM
CP
DPS
TSM
NP
PST
PS
VSM
AS
OSM
QAM
PERI
MF
MT
1C
CANM
CAOM
CATM
CAUM
CAWM
CAXM
EA
PROBE TIP DIAMETER
NET TINF. OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL» DRY
PERCENT 02 BY VOL» DRY
PERCENT CO BY VOL» DRY
PERCENT N2 BY VOL » DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
MET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE* DRYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAD-PTLtSTD CN
PART. LOAD-TTL»STD CN
PART. LOAD-PTL.STK CM
PART. LOAO-TTL«STK CN
PARTIC EMIS-PARTIAL
PARTIC FMIS-TOTAL
PERCENT EXCESS AIR
IN
MIN
IN.HG
IN.H20
DCF
OEG.F
NCM
ML
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
M3/MIN

MG
MG

MG/NM3
MG/NM3
MG/M3
MG/M3
KG/HR
KG/HP

.600
30.0
29.26
.442
11.35
68.4
.32
31.0
.04
11.6
.884
11.0
9.2
1.9
77.9
30.13.
28.72
.850
.007
11.1
6
-0.00
29.26
83.8
11,3101'
5 47 */
612*7
76.7
786.70
955.70
17.68
2487.49
3021.85
2224.82
2702.75
82
99
67
.600
240.0
29.31
.506
96.34
75.5
2.6S
675.2
.91
25.5
.745
11.0
9.2
1.9
77.9
30.13
27.04
.850
.008
f.S.8
48
-0.00
29.31
101.2
29
1.2
1.9
94.0
2162.50
4855.10
55.46
814.79
1829.31
516.25
1159.06
.058k/
.13ll/
f>7
.600
160.0
29.31
.539
67.08
79.8
1.83
5^8.0
.80
30.5
,695
15.0
7.3
2.9
74.8
30.69
26.82
.850
.008
70.1
32
-0.00
29.31
107.7
29
1.2
2.0
99.5
3178.70
9264.70
65.69
1733.81-)
5053.51
1011.99
2949.56
.nik/
.354k/
4?
 aj  Nominal  10-ft (120 in.) diameter stack.
 b/  Per stackj to obtain total for kiln, multiply by 8.
                                    62

-------
                           TABLE A-10   (Continued)

                       PARTICULATE EMISSION DATA
                              (METRIC RESULTS)
          DESCRIPTION
       DATE OK RUN
UNITS
11
         12-05-75   12-06-75   12-07-75
ON
TT
PB
PM
VM
TM
VMSTM
VW
VWM
PMOS
MO
PC02
P02
PCO
PN2
MWD
MM
CP
DPS
TSM
NP
PST
PS
VSM
AS
QSM
QAM
PERI
MF
HT
1C
CANM
CAOM
CATM
CAUM
CAWM
CAXM
EA
PROBE TIP DIAMETER
NET TIKE OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY 6AS-STD COND
TOTAL H2G COLLECTED
VOL H«:0 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL* DRY
PERCENT 02 BY VOL« DRY
PERCENT CO BY VOL » DRY
PERCENT N2 hY VOL* DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE, ABSOLUTE
AVG STACK CAS VELOCITY
STACK AREA
STK FLOWRATEi DRY,STD CN
ACTUAL STACK FLOwRATE
PERCENT ISOKINF.TIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINIJER CATCH
PART. LOAU-PTL.STO CN
PAHT. LOAO-TTLISTD CN
PART. LOAD-PTL. ,STK CN
PART. LOAD-TTL»STK CN
PARTIC ECUS-PARTIAL
PART 1C I: MIS-TOTAL
PERCENT EXCESS AIH
IN
MIN
IN.HG
IN.H20
DCF
DEG.F
NCM
ML
NM3









IN.H20
OEG.C

IN.HG
IN.HG
M/MIN
IN?
NM3/MIN
M3/MIN

MG
MG

MG/NM3
MG/NM3
MG/M3
MG/M3
KG/HR
KG/HR

.600
160.0
29.25
.412
57.24
79. B
1.56
624.7
.84
35.0
.650
17.2
9.2
4.1
69.5
31.12
26.53
.aso
.0.06
73.8
32
-0.00
29.25
94.3
29
.9
1.8
104.6
10536.20
62150.60
83.05
6751.16
39823.53
3638.97
21465.44
.3B3&.
2.257-'
64
.600
105,0
29.65
.350
34.18
53.3
.99
316.4
.42
30.0
.700
16.1
6.4
1.5
76.0
30.83
26.98
.850
.006
69.5
21
-0.00
29.65
89.3
29
1.0
1.7
97.0
3719.50
6569.10
56.59
3744.88
8627.56
2231.09
5140.06
.222^
.512k/
39
.600
120.0
29.65
.319
37.53
54.4
1.09
370.0
.50
31.4
.686
IB. 2
5.1
5.5
71.2
31.12
27.00
.850
.006
94.8
24
-0.00
29.65
91.5
29
.9
1.7
99.4
6043.60
12969.50
53.40
5553.14
11916.98
3020.04
6480.97
•308t/
.661^
14
_a/  Per stack;  to obtain total for kiln, multiply by 8,
b/  Per stack;  to obtain total for kiln, multiply by 7.
                                   63

-------
                        TABLE A-10  (Concluded)

                          PARTICULATE EMISSION DATA
                                 (METRIC RESULTS)
 NAME       DESCRIPTION

        DATE  OF HUN
UNITS       13         U

         12-08-75   12-08-75
DN
TT
PB
PM
VM
TM
VMSTM
VM
VWM
PMOS
MD
PC02
P02
PCO
PN2
MUD
MW
CP
DPS
TSM
NP
PST
PS
VSM
AS
QSM
QAM
PERI
MF
MT
1C
CANM
CAOM
CATM
CAUM
CAWM
CAXM
EA
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOLt DRY
PERCENT 02 BY VOLt DRY
PERCENT CO BY VOLt DRY
PERCENT N2 BY VOLt DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSUREt ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATEt DRYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAD-PTLtSTD CN
PART, LOAO-TTLtSTD CN
PART. LOAD-PTLtSTK CN
PART. LOAD-TTLtSTK CN
PARTIC EMIS-PARTIAL
PAKTIC EM1S-TOTAL
PERCENT EXCESS AIR
IN
MIN
IN.HG
IN.H20
DCF
DEG.F
NCM
ML
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
M3/MIN

MG
MG

MG/NM3
MG/NM3
MG/M3
MG/M3
KG/HR
KG/HR

.600
25.0
29. 35
.180
5,62
44.8
.16
52.5
.07
30.1
.699
22.3
1.1
6.7
69.9
31.61
27.52
.850
.004
158.3
5
-0.00
29.35
85.4
29
.7
1.6
89.7
1577.80
2566,30
38.52
9601.92
15617.58
4493.69
7309.01
.428£/
.6 95 */
-11
.600
70.0
29.35
.207
16.41
48.0
.46
176.0
.24
33.2
.668
22.3
1.1
6.7
69.9
31.61
27.10
.850
.004
145.3
14
-0.00
29.35
79,3
29
.7
1,5
101,7
6856.70
10048.90
31.75
14383.35
21073.51
6631,29
9715.72
.586^7
.858^
-11
£/  Per stack;  to obtain total, multiply by 1.67.
b_/  Per stack;  to obtain total for kiln, multiply by 7.
                                64

-------
                                                TABLE A-11
                                      SUMMARY OF  RESULTS (PARTICIPATE)
Ul
              NAME       DESCRIPTION

                      HATE OF RUN
UNITS      I           3          5

         12-02-75   12-03-75   12-04-75
VMSTD VOL DRY GA.S-STD COND
PMOS
TS
OS
OA
PERI
PART
MF
CAN
CAT
CAW
PART
MT
CAO
CAU
CAX
1C
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE, DRYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
ICULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAD-PTL,STD CN
PART. LOAD-PTL,STK CN
PARTIC EMIS-PARTIAL
ICULATES — TOTAL CATCH
PARTICULATE WT-TOTAL
PART. LOAD-TTL»STD CN
PART. LOAO-TTL»STK CN
PARTIC F.MIS-TOTAL
PERC IMPINGER CATCH
DSCF

DEG.F
DSCFM
ACFM


MG
GR/DSCF
GR/ACF
LB/HR

MG
GR/DSCF
GR/ACF
LB/HR

DSCF

DEG.F
DSCFM
ACFM

11.15
11.6
5P.O
11,310£/
21,60l£/
76.7
93.53
25.5
150.5
4?
66
94.0
64.61
30.5
158.3
41
71
99.5
MG
GR/DSCF
GR/ACF
LB/HR
786.70
1.08703
.97224
180
2162.50
.35606
.22560
.13—'
3178.70
.75769
.44224
.27—
 955.70
1.32054
1.18110
     219
  17.60
                                                                       4855.10
                                                                        .79940
                                                                        .50651
                                                                         55.46
               a/  Based on nominal 10-ft (120 in.) diameter stack.
               b/  Per stack; to obtain total for kiln, multiply by 8.
                                9264.70
                                2.20837
                                1.28895
                                  65.69

-------
                               TABLE A-ll   (Continued)

                          SUMMARY OF RESULTS (PARTICULATE)
NAME

DESCRIPTION
DATE OF RUN
VMSTD VOL DRY GAS-STD COND
PMOS
TS
OS
OA
PERI
PART
MF
CAN
CAT
CAW
PART
MT
CAO
CAU
CAX
1C
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE. DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
ICULATES — PARTIAL CATCH
PARTICULAR WT-PARTIAL
PART. LOAD-PTL»STD CN
PART. LOAD-PTL,STK CN
PARTIC EMIS-PARTIAL
ICULATES — TOTAL CATCH
PARTICULATE WT-TOTAL
PART. LOAD-TTL.STD CN
PART. LOAD-TTL»STK CN
PARTIC LMIS-TOTAL
PERC IMPINGER CATCH
UNITS

DSCF

DEG.F
DSCFM
ACFM


MG
GR/DSCF
GR/ACF
LB/HR

MG
GR/DSCF
GR/ACF
LB/HR

7
12-05-75
55.00
35.0
164.8
33
62
104.6

10536.20
2.95024
1.59022
.84£/

62150.60
17.40280
9.38035
83.05
9
12-06-75
35.00
30.0
157.1
35
59
97.0

3719.50
1.63650
.97498 ,
.49E/

8569.10
3.77023
2.24620
56.59
11
12-07-75
38.35
31.4
202.7
33
60
99.4

6043.60
2.42671
1.31975
.68£/

12969.50
5.20770
2.83217
1.46£/
53.40
aj  Per stack;  to obtain total for kiln, multiply by 8.
b/  Per stack;  to obtain total for kiln, multiply by 7.

-------
                           TABLE A-11   (Concluded)

                      SUMMARY OF RESULTS  (PARTICIPATE)
NAME

DESCRIPTION
DATE OF RUN
VMSTD VOL DRY GAS-STD COND
PMOS
TS
QS
QA
PERI
PART
MF
CAN
CAT
CAW
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATEt DRYtSTD CN
ACTUAL' STACK FLOWRATE
PERCENT ISOKINETIC
ICULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAD-PTLtSTD CN
PART. LOAD-PTL'»STK CN
PARTIC EMIS-PARTIAL
UNITS

DSCF

DEG.F
DSCFM
ACFM


MG
GR/DSCF
GR/ACF
LB/HR
13
12-08-75
5.79
30.1
317.0
26
56
89.7

1577.80
4.19602
1.96373
.94£/
14
12-08-75
16.80
33.2
293.6
24
52
101.7

6858.70
6.28550
2.89786
1.29k/
PARTICULATES — TOTAL CATCH
MT
CAO
CAU
CAX
1C
PARTICULATE WT-TOTAL
PART. LOAD-TTL»STD CN
PART. LOAO-TTL»STK CN
PARTIC EMIS-TOTAL
PERC IMPINGER CATCH
MG
GR/DSCF
GR/ACF
LB/HR

2566.30
6.82485
3.19402
1.53£/
38.52
10048.90
9.20908
4.24575
1.89k/
31.75
a/  Per stack; to obtain total, multiply by 1.67.
b/  Per stack; to obtain total for kiln, multiply by 7.

-------
                                                      TABLE A-12
                                    SUMMARY OF RESULTS—METRIC UNITS (PARTICULATE)
oo
NAME

VMSTM
PMOS
TSM
QSM
QAM
PERI
EA
PARTI
MF
CANM
CATM
CAWM
PARTI
MT
CAOM
CAUM
CAXM
1C
DESCRIPTION
DATE OF RUN
VOL DRY GAS-STD COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE* ORY»STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PERCENT EXCESS AIR
CULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAD-PTL.STD CN
PART. LOAD-PTL»STK CN
PARTIC EMIS-PARTIAL
CULATES — TOTAL CATCH
PARTICULATE WT-TOTAL
PART, LOAO-TTL»STD CN
PART. LOAO-TTL»STK CN
PARTIC EMIS-TOTAL
PERC IMPINC3ER CATCH
UNITS

NCM

OEG.C
NM3/MIN
M3/MIN



MG
MG/NM3
MG/M3
KG/HR

MG
MG/NM3
MG/M3
KG/HR

1
12-02-75
.316
11.6
11.1 ,
547£/
6122/
76.7
67

786.70
2487.49
2224.02
82

955.70
3021.85
2702.75
99
17.68
3
12-03-75
2.649
25.5
65.8
1.2
1.9
94.0
67

2162.50
814.79
516.25
..058k/

4855.10
1829.31
1159.06
.13li/
55.46
5
12-04-75
1.B29
30.5
70.1
1.2
2.0
99.5
42

3170.70
1733.85
1011.99
,12lW

9264.70
5053.51
2949.56
.354^7
65.69
                a/   Nominal  10-ft  (120  in.)  diameter stack.
                b/   Per stack;  to  obtain total  for kiln,  multiply by 8.

-------
                               TABLE A-12   (Continued)

                    SUMMARY  OF RESULTS—METRIC UNITS  (PARTICULATE)
NAME DESCRIPTION UNITS
DATE OF RUN
VMSTM VOL DRY GAS-STO COND NCM
PMOS PERCENT MOISTURE BY VOL
TSM AVG STACK TEMPERATURE DEG.C
QSM STK FLOWRATE* DRY.STD CN NM3/MIN
QAM ACTUAL STACK FLOWRATE M3/MIN
PERI PERCENT ISOKINETIC
EA PERCENT EXCESS AIR
PART
MF
CANM
CATM
CAWM
PART
MT
CAOM
CAUM
CAXM
1C
ICULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAO-PTL.STO CN
PART. LOAO-PTL»STK CN
PARTIC FMIS-PARTIAL
ICULATF.S — TOTAL CATCH
PARTICULATE WT-TOTAL
PART. LOAD-TTLfSTD CN
PART. LOAD-TTL.STK CN
PARTIC F.MIS-TOTAL
PERC IMPINGER CATCH

MG
MG/NM3
MG/M3
KG/HR

MG
MG/NM3
MG/M3
KG/HR

7
12-05-75
1.557
35.0
73.8
.9
1.8
104.6
64

10536.20
6751.16
3638.97
.383£/

62150.60
39823.53
21465.44
2.257£/
83.05
9
12-06-75
.991
30.0
69.5
1.0
1.7
97.0
39

3719.50
3744.88
2231.09
.2 22^7

8569.10
8627.56
5140.06
.512k/
56.59
11
12-07-75
1.086
31.4
94.8
.9
1.7
99.4
14

6043.60
5553.14
3020.04
.308£/

12969.50
11916.98
6480.97
.661*/
53.40
a/  Per stack; to obtain total for kiln,  multiply by 8.
b/  Per stack; to obtain total for kiln,  multiply by 7.

-------
•-J
o
                                                TABLE A-12   (Concluded)



                                    SUMMARY OF  RESULTS—METRIC UNITS  (PARTICULATE)
NAME

DESCRIPTION
DATE OF RUN
VMSTM VOL DRY GAS-STD COND
PMOS
TSM
QSM
QAM
PERI
EA
PART
MF
CANM
CATM
CAWM
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATEt DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PERCENT EXCESS AIR
ICULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAD-PTLtSTD CN
PART. LOAD-PTLtSTK CN
PARTIC EMIS-PARTIAL
UNITS

NCM

DEG.C
NM3/MIN
M3/MIN



MG
MG/NM3
MG/M3
KG/HR
13
12-08-75
.164
30.1
158.3
.7
1.6
89.7
-11

1577.80
9601.92
4493.69
,428^/
14
12-08-75
.476
33.2
145.3
.7
1.5
101.7
-11

6858.70
14383.35
6631.29
.586^'
PARTICULATES — TOTAL* CATCH
MT
CAOM
CAUM
CAXM
1C
PARTICULATE WT-TOTAL
PART. LOAD-TTU»STD CN
PART. LOAD-TTL.STK CN
PARTIC EMIS-TOTAL
PERC IMPINGER CATCH
MG
MG/NM3
MG/M3
KG/HR

2566.30
15617.58
7309.01
.695£/
38.52
10046.90
21073.51
9715.72
.858^'
31.75
                        a/  Per stack; to obtain total, multiply by 1.67.

                        b/  Per stack; to obtain total for kiln, multiply by 7.

-------
    APPENDIX B
SAMPLE CALCULATIONS
        71

-------
                                   EXAMPLE PARTICULATE  CALCULATIONS
ro
1.  VOLUME OF OPY GAS SAMPLED AT STANDARD  CONDITIONS     (1)


                 17.71*VM»(PB + PM/13.6)
       VMSTD =  	
        	-	- —-	J-M + 460. 	             ....  . _

                17.71* 57.24*(29.25*   .412/13.6)
        	  =  	^-	=     55.00 DSCF
                         79.8*460.

      .VMSTM =_. VMSTO^O.028317=   55.00*0.028317=      1.56 DNM3


2.  VOLUME OF WATER VAPOR AT STANDARD  CONDITIONS


       VWV 	=	0.0474*V*'	= -0.0474*-624.7      =     29.61 SCF

       VWK   =  VWV«0.028317 = 29.611*0.028317   =     .8385 NM3


3.  PERCENT MOISTURE IN  STACK GAS


                  100.*VWV      100.«  29.61
       PMOS  =  —	•-— s....	     =.      35.0 PERCENT
                 VMSTD*VWV      55.00*  29.61

-------
                  4.  MOLE FRACTION  OF  DRY STACK GAS
                         MD
 1GO.-PMOS
»«VM«»«WM«»«BM««^

...'. 400.	
 100.-    35.0
lflV«»«W^^«»«»^«»^«»«

	 100.
.650
CO
                  5.  .AVERAGE MOLECULAR- WEIGHT OF-DRY STACK GAS

                         MWD   =   (PC02 « 44/100) + (P02 * 32/100)
                  		  	*-(PN2+PCO.-..« 28/100-)	
                                   (17.2  * 44/100) * ( 9.2 « 32/100)
                                       +473.6 * 28/100)
                  6.  MOLECULAR  WEIGHT  OF STACK GAS
                                                                          31.12
                         MM     =   MrtD«MD * 18»(1-MD>

                                =    31.1* ,.650 > 18«(1- .650)
                                       26.53

-------
7.  STACK GAS VELOCITY  AT  STACK  CONDITIONS
             =  5129*CP*ASQRT(DPS*(TS+460))*
                    SORT(1/(PS*MW))

             =  5129*   .850  *   1.977
                   "SORT(1/129.25*   26.53))
       VSM   =  VS*0.3048   a
309*0.3048
309 FPM

 94 METERS/MIN
6.  STACK GAS VOLUMETRIC  FLOW  AT STANDARD CONDITIONS*  DRY  BASIS


                  0.123*VS»AS»MO*PS
       OS    =  	
       .  —  —. 	T-S*460-			--	      	-

                  0.123«    309*    29» .650*29.25
           .	ir.  ^. T*** ™^** •^*^»."*^«»*»^^^«»^«"^i^«p«*^^^^«w^"»^«»^^..
                          164.8 +460
                                                 =        33 DSCFM

       QSM   =  QS*0.028317  =       33«0.028317  =          1 NM3/MIN


9.  STACK GAS VOLUMETRIC  FLOW  AT STACK CONDITIONS


                  OS  *  (TS+460)
       QA    =  	
     		17..71-»-.P-S  •»  -MO	 -	

                      33
-------
               10.   PERCENT -ISOKINE.TIC
01
     		1D32
-------
13.
     PAKTICULATE LOADING — PROBE* CYCLONE*  AND  FILTER
      	-IAT--STACK CONDITIONS)
       CAT
                 17.71*CAN*PS»MD
                     TS+460
       -   		17,71* a.2390*29.25* -,650
                       164.8+460
       CATM  =  CAT*2288.34 =   1.20683»2288.34    =   2761.64 MG/M3
                                                 =  1.20683 GR/ACF
14.  PAP-TICULATE LOADING — TOTAL
                     (AT STACK CONDITIONS)
       CAU
                                                 =  7.25071 GR/ACF
                  17.71*CAO*PS«MD
                     TS+460
   	_..	-17,71«13^4518#29.25*. .650	
                        164.8+460
       CAUM   =  CAU*2288.34  =   7.25071*2288.34    *  16592.09 MG/M3
15.   PARTICULATE EMISSION RATE
                     — PR08E» CYCLONE, AND FILTER
      CAW    =   0.00857»CAN»OS
             =   0.00857«   2.2390»       33
      CAWM   =   CAW*0.45359  =      ,64«0.45359
                                                         .64 LH/HH
                                                         .?9 KG/HP

-------
16.   PARTICULATE  EMISSION RATE
                     ~ TOTAL
       CAX   «*  0.00857*CAO*QS

             =  0.00857* 13.4518*      33

       CAXM  =  CAX*0.45359 =    3.85*0.45359


17.   PERCENT EXCESS AIR AT SAMPLING POINT
       EA
 100. « (P02-0.5*PCO)

0.264«PN2-P02+0.5»PCO

 100. M 9.2-0.5* 4.1)

0.264*69.5- 9.2*0.5* 4.1
                                        3.B5 LR/HR

                                        1.74 KG/HR
                                                       63.9 PERCENT
(1)   STANDARD CONDITIONS- AT 70 DEO F (21.1 DEG C), 29.92 IN HG  (760 MM HG)

-------
                APPENDIX C
RESULTS OE; ANALYSIS - COMPUTER COMPUTATIONS
              (TOTAL ORGANIC)
                    78

-------
                                               TABLE C-l
                                    ORGANIC DATA AND CALCULATED VALUES
vo
         ATMOS  ATMOS   STACK    H20
         TEMP   PRES     VAC    CONO
        (06.F)  (I.HG)  (I.H20)  (ML)
         60.0   39.26    0.00    31.0   554.90   646.70
UN- 1
PARTIC
WT-PTL
(M6)
DATE-
PARTIC
WT-TTL
(MG)
12-02-75
STACK IN1T
AREA VOL
(FT2) (DCF)
       PERC PERC  PERC PITOT
        02   C02   CO   TUBE
        DRY  DRY   DRY  COEF
601.61  9.2  11.0   1.9
,850
PORT-
POINT

1
D
D
D
D
D
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
802.84
804.15
806.04
808.02
810.29
812.96
DELTA
P
I.H20)
.002
.008
.008
.008
.008
.008
DELTA
H
(I.H20)
• 150
.250
.400
.450
.550
.850
TEMP
IN
(D.F) -(
62.0
64.0
67.0
72.0
80.0
85.0
TEMP
OUT
;D.F)
62.0
64.0
64.0
64.0
68.0
69.0
TRAIN
VAC
(I.HG)
1.0
1.0
2.0
2.5
4.0
5.5
STACK
TEMP
(D.F)
62.0
50.0
50.0
50.0
50.0
50.0
S.GEL PROBE
TEMP T OIA
(D.F) (IN)
.600
.600
.600
.600
.600
.600

VEL
(FPM)
150.0
300.0
300.0
300.0
300.0
300.0

-------
                                               TABLE C-2
                                    ORGANIC DATA AND CALCULATED VALUES
                                   RUN-
 DATE- 12-03-75
         ATMOS  ATMOS  STACK   H20     PARTIC
         TEMP   PRES    VAC   COND     WT-PTL
        (D6.F) (I.HG)  (I.H20) (ML)      (MO)
PARTIC  STACK   INIT
WT-TTL   AREA    VOL
 (MG)   (FT2)   (DCF)
         40.0   29.31   0.00  675.2   1574.60  3367.30
PERC PERC PERC  PI TOT
 02   C02   CO    TUBE
 DRY  DRY   DRY   COEF
          • 20   813.01   9.2 11.0  1.9   .8
-------
00
                                           TABLE C-2  (Continued)




                                     RUN-    3      DATE- 12-03-75
PORT-
POINT

4
4
4
3
3
3
3
3
3
5
5
5
5
5
5
6
6
6
6
6
6
7
7
7

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
842.42
844.38
846.64
848.58
850.39
852.26
854.17
856.33
858.82
860*99
863.59
866.03
868.03
870,31
872.79
875.34
878.03
880.37
882.08
884.03
886.24
888.17
889.99
891.61
DELTA
P
I.H20) (
.007
.009
.009
.006
.006
.008
.008
.009
.009
.011
.011
.008
.008
.014
.014
.011
.011
.006
.006
.008
.008
.006
.006
.005
DELTA
H
I.H20)
.400
.500
.550
.500
.400
.450
.400
.500
.700
.700
.750
.700
.600
.750
.700
.750
.800
.800
,550
,550
.650
.550
.450
.400
TEMP
IN
(D.F)
80.0
85.0
87.0
65.0
70.0
80.0
83.0
81.0
87.0
76.0
82.0
95.0
94.0
98.0
100.0
82.0
89.0
98.0
98.0
98.0
100.0
86.0
90.0
95,0
TEMP
OUT
(D.F)
65.0
66.0
68.0
66.0
66.0
67.0
68.0
70.0
72.0
73.0
74.0
75.0
76.0
77.0
78.0
78.0
79.0
80.0
80.0
81. 0
82.0
82.0
82.0
82.0
TRAIN
VAC
(I.HQ)
6.5
8.0
9.0
11.0
11.0
14.0
15.0
6.0
6.0
6.0
7.5
7.5
8.0
10.0
14.0
6.0
7.0
7.0
7.0
8.0
10.0
8.0
8.0
10.0
STACK S.GEL
TEMP TEMP

-------
                                           TABLE C-2  (Concluded)
                                     RUN-
DATE-  12-03-75
oo
PORT- SAMP METER DELTA
POINT TIME VOL P
(MIN) (DCF) (I.H20) (
7 1 5.00 893.37 .005
7 1 5.00 894.87 .004
7 1 5.00 896.38 .004
8 1 5.00 898.77 .011
8 1 5.00 901.12 .011
8 1 5.00 903.36 .008
8 1 5.00 905.49 .008
8 1 5.00 907.40 .007
8 1 5.00 909.35 .007
DELTA TEMP TEMP TRAIN STACK S.GEL PROBE
H IN OUT VAC TEMP TEMP T DIA VEL
I.H20) (D.F) (D.F) II. HG) (D.F) (O.F) (IN) (FPM)
.400 97.0 83.0 11.0 155.0 .600 280.0
.300 100.0 84.0 12. 0 155.0 .600 250.0
.300 98.0 84.0 13.0 155.0 .600 250.0
.650 82.0 81.0 6.0 165.0 .600 400.0 £&»
.650 87.0 82.0 6.5 165.0 .600 400.0 J™!
.550 95.0 82.0 7.0 160.0 .600 350.0 SQI
ecn ax. t\ ay n 7 « n IftOaO .600 350.0 maim. 	
.550 96.0 oc.O i.u lou.w .w«w ~> nwBB^8l
.400 99.0 82.0 7.0 160.0 55.0 .600 320.0 g^^i
* "r U U ^y»v ^**-wv _,»— -1 -^ rt n ri7u»u<.jLfti«i««MH
.400 99.0 82.0 7.0 160.0 .600 320.0 m&BBt
™ 9

-------
                                                       TABLE C-3
                                          ORGANIC DATA AND CALCULATED VALUES
oo
ATMOS
TEMP
(DG.F)
50.0
PORT-
POINT

1 1
1 1
1 1
1 1
2 1
2 1
2 1
2 1
4 1
4 1
4 1
4 1
3 1
3 1
3 1
3 1
ATMOS
PRES
(I.HG)
29.31
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
911.14
912.85
914.55
916.25
918.28
920.33
922.34
924.53
926.59
928.65
930.73
932.78
934.63
936.39
938.42
940.55
RUt»- 5
H?0 PARTIC
COND WT-PTL
(ML)
598.0
DELTA
P
I.H20)
.006
.006
.006
.006
.008
.008
.008
.008
.008
.008
.008
.008
.006
.006
.008
.008
(MG)
2515.50
DELTA
H
(I.H20)
.450
.400
.400
.350
.550
.550
.500
.600
.550
.500
.500
.500
.400
.400
.500
.500
DATE- 12-04-75
PARTIC STACK
WT-TTL AREA
(MG) (FT2)
6815
TEMP
IN
(D.F)
54.0
58.0
66.0
68.0
66.0
72.0
83.0
86.0
75.0
80.0
90.0
92.0
79.0
83.0
90.0
93.0
.40
TEMP
OUT
(D.F)
56.0
56.0
56.0
57.0
62.0
62.0
65.0
65.0
70.0
72.0
74.0
74.0
76.0
77.0
78.0
79.0
.20
TRAIN
VAC
(I.HG)
5.0
5.5
5.5
6.0
8.0
10.0
10.5
11.0
11.0
11.0
12.0
12.0
5.0
5.0
6.0
6.0
INIT
VOL
(DCF)
909.35
STACK
TEMP
(D.F)
155.0
155.0
155.0
150.0
150.0
150.0
145.0
145.0
155.0
160.0
160.0
160.0
155.0
160.0
160.0
160.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY DRY COEF
7.3 15.
0 2.
9 .850
S.GEL PROBE
TEMP T
DIA
(D.F) (IN)
•
«
55.0 ,
.
.
•
.
.
.
.
65.0 .
•
.
•
65.0 .
•
600
600
600
600
600
600
600
600
600
600
600
600
600
600
600
600
VEL
(FPM)
300.0
300.0
300.0
300.0
350.0
350.0
350.0
350.0
350.0
350.0
350.0
350.0
300.0
300.0
350.0
350.0

-------
                                              TABLE C-3  (Concluded)
                                       RUN-
DATE-  12-04-75
00
-p-
PORT-
POINT

5
5
5
5
6
6
6
6
7
7
7
7
8
8
6
8

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF)
9*2.89
945.26
947.63
950.01
952.39
954.77
957.19
959.60
961.40
963.18
964.95
966.73
969.13
971.54
973.93
976.43
DELTA
P
(I.H20)
.011
.011
• Oil
.011
.011
.011
.011
.011
.006
.006
.006
.006
.011
• Oil
.011
.011
DELTA
H
(I.H20)
.700
.700
.650
.650
.700
.650
.700
.700
.500
.400
.350
.300
.650
.650
.650
.650
TEMP
IN
(D.F)
73.0
79.0
91.0
95.0
83.0
90.0
100.0
103.0
86.0
89.0
95.0
97.0
90.0
96.0
104.0
108.0
TEMP
OUT
(D.F)
65.0
75.0
76.0
77.0
80.0
81.0
83.0
83.0
84.0
85.0
86.0
87.0
86.0
88.0
88.0
90,0
TRAIN
VAC
(I.HG)
6.0
7.5
9.0
9.0
10.0
11.0
11.5
12.0
5.0
5.0
5.5
6.5
10.0
10.5
11.5
12.0
STACK S.GEL
TEMP TEMP
(D.F) (D.F)
160.0
155.0
160.0
160.0
160.0
160.0
165.0
160.0
165.0
165.0
165.0 65.0
165.0
165.0
165.0
160.0
160.0
PROBE
T DIA
(IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600

VEL
(FPM)
400.0
400.0
400.0
400.0
400.0
400.0
400.0
400.0
300.0
300.0
300.0
300.0
400.0
400.0
400.0
400.0

-------
                                               TABLE C-4
                                    ORGANIC DATA AND CALCULATED VALUES
                                   RUN-
 OATE-  12-05-75
         ATMOS  ATMOS  STACK   H20     PART 1C
         TEMP   PKES    VAC   COND     WT-PTL
        (OG.F) (I.HG) (I.H20) (ML)      (MG)
PARTIC  STACK   INIT
WT-TTL   AREA    VOL
 (MG)   (FT?)   (OCF)
         50.0   29.25   0.00  624.7   7996.00 48040.40
PERC PERC PFRC  PITOT
 02   C02  CO    TUBE
 DRY  DRY  DRY   COEF
           .20   977.30   9.2 17.2  4.1   .850
oo
PORT-
POI

1
1
1
1
2
2
2
2
4
4
4
4
3
3
NT

1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
978.81
980.18
901.61
983.08
984.80
986,52
988.47
990.56
992.31
994.20
995.95
997.72
999.19
1000.66
DELTA
P
I.H20)
.004
.004
.004
.004
.006
.006
.008
.008
.006
.006
.006
.006
.004
.004
DELTA
H
(I.H20)
.300
.250
.250
.250
.350
.300
.400
.500
.350
.450
.400
.400
.300
.250
TEMP
IN
(D.F)
64.0
6fl.O
72.0
74.0
72.0
77.0
85.0
88.0
78.0
81.0
90.0
92.0
80.0
82.0
TEMP
OUT
(D.F)
66.0
67.0
67.0
68.0
70.0
71.0
73.0
74.0
76.0
77.0
78.0
79.0
HO.O
80.0
TRAIN
VAC
(I.HG)
4.0
4.0
4.0
4.0
5.0
6.0
8.0
8.5
10.0
11.0
12.0
12.0
4.0
5.0
STACK
TEMP
(D.F)
155.0
155.0
150.0
150.0
155.0
150.0
150.0
150.0
165.0
160.0
165.0
160.0
160.0
160.0
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
60.0 .600
.600
.600
.600
65.0 .600
.600
.600
.600
.600
.600
.600
.600

VEL
(FPM)
250.0
250.0
250.0
250.0
300.0
300.0
350.0
350.0
300.0
300.0
300.0
300.0
250.0
250.0

-------
oo
                                           TABLE C-4  (Concluded)




                                    RUM-    7      DATE-  12-05-75
PORT-
POINT

3
3
5
5
5
5
6
6
6
6
7
7
7
7
8
8
8
8

1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(OCF) (]
1002.10
1003.49
1005.43
1007.39
1009.53
1011.61
1013.61
1015.64
1017.64
1019.41
1021.70
1023.97
1026.25
1028.50
1029.96
1031.42
1032.96
1034.54
DELTA
P
I.H20) (
.004
.004
.008
.008
.008
.008
.008
.008
.007
.007
.010
.010
.010
.010
.004
.004
.005
.005
DELTA
H
I.H20)
.250
.250
.450
.450
.550
.550
.550
.500
.450
.350
.700
.700
.650
.650
.400
.400
.300
.300
TEMP
IN
(D.F)
88.0
90.0
70.0
74.0
84.0
87.0
77.0
83.0
92.0
94.0
84.0
92.0
98.0
103.0
80.0
81.0
86.0
89.0
TEMP
OUT
(D.F)
81.0
82.0
74.0
74.0
74.0
75.0
77.0
78.0
79.0
80.0
80.0
82.0
83.0
84.0
80.0
81.0
82.0
81.0
TRAIN
VAC
(I. HO)
5.0
6.0
9.0
10.0
11.0
11.0
5.0
9.0
10.0
9.0
12.0
12.0
12.0
12.5
5.0
9.0
9.0
9,0
STACK S.GEL
TEMP TEMP
(D.F) (O.F)
160.0 60.0
160.0
160.0
165.0
165.0
170.0
170.0
165.0
160.0
165.0
185.0
185.0
190.0
185.0
180.0
175.0
175.0
175.0
PROBE
T DIA
(IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
VEL
(FPM)
250.0
250.0
350.0
350.0
350.0
350.0
350.0
350.0
325.0
325.0
400.0
400.0
400.0
400.0
250.0
250.0
275.0
275.0

-------
                                                    TABLE G-5
                                        ORGANIC^DATA AND CALCULATED VALUES
                                      RUN-
DATE-  12-06-75
oo
ATMOS
TEMP
DG.F)
40.0
PORT-
POINT

4 1
4 1
4 1
3 1
3 1
3 1
5 1
5 1
5 1
6 1
6 1
6 1
ATMOS
PRES
(I.HG)
29.65
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
U.H20)
0.00
METER
VOL
(DCF) (
36.12
37.68
39.44
41.12
42.73
44.51
46.19
47.87
49.55
50.96
52.36
53.76
H?0
COND
(ML)
316.4
DELTA
P
I.H20)
.006
.006
.006
.006
.006
.006
.006
.006
.006
.004
.004
.004
PARTIC
WT-PTL
(MG)
2855.50
DELTA
H
(I.H20)
.300
.350
.400
.400
.400
.400
.400
.400
.350
.250
.250
.250
PARTIC STACK INIT
WT-TTL AREA VOL
(MG) (FT2)
6491
TEMP
IN
(D.F)
40.0
43.0
49.0
4fl.O
51.0
57.0
51.0
55.0
60.0
54.0
58.0
60.0
.20
TEMP
OUT
(D.F)
40.0
41.0
42.0
45.0
46.0
47.0
50.0
50.0
51.0
52.0
52.0
53.0
.20
TRAIN
VAC
(I.HG)
4.0
5.0
6.5
8.0
8.0
9.0
9.0
9.5
10.0
10.0
10.5
11.0
(DCF)
34.54
STACK
TEMP
(D.F)
155.0
160.0
160.0
145.0
145.0
145.0
150.0
155.0
155.0
150.0
155.0
155.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY DRY COEF
6.4 16.1 1
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.5 .850

VEL
(FPM)
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
250.0
250.0
250.0

-------
                                        TABLE C-5  (Concluded)

                                  RUN-    9     DATE- 12-06-75
oo
oo
PORT-
POINT

7
7
7
8
8
8
1
1
1

1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF)
55.53
57.10
58.69
60. 44
62.05
63.70
65.39
67.09
68.72
                              DELTA
                                P
                            (I.H20)
.006
.006
.006
.006
.006
.006
.006
.006
.006
ELTA
H
H20)
.400
.350
.300
.400
.350
.350
.350
.350
.350
TEMP
IN
(D.F)
55.0
59.0
63.0
54.0
58.0
63.0
60.0
64.0
68.0
TEMP
OUT
(D.F)
54.0
55.0
55.0
55.0
56.0
56.0
56.0
56.0
58.0
TRAIN
VAC
(I.HG)
4.0
5.0
7.5
13.0
13.0
12.0
11.0
12.5
13.0
STACK
TEMP
(D.F)
165.0
165.0
165.0
165.0
170.0
170.0
155.0
155.0
160.0
                                        TEMP  T  DIA
                                       (D.F)  (IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
       VEL
      (FPM)
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0
300.0

-------
                                       TABLE C-6
                            ORGANIC DATA AND CALCULATED VALUES
                          RUM-    11
 PATF.- 12-07-75
 ATMOS  ATMOS  STACK   H20    PARTIC
 TEMP   PRES    VAC   CONO    WT-PTL
(DG.F) (I.HG) (I.H20) (ML)      (MG)
PARTIC  STACK
WT-TTL   AREA
 (MG)   (FT2)
 40.0   29,65   0.00  370.0  4777.90   8821.20
           ,20
INIT   PERC PERC PERC  PITOT
 VOL    02   C02   CO    TUBE
(DCF)   DRY  DRY   DRY   COEF

 70.83  5.1 18.2   5.5   .850
PORT-
POINT

1
1
1
4
4
4
3
3
3
5
5
5

1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (1
72.13
73.50
74.86
76.66
78.44
80.25
81.87
83.43
84.83
86.49
88.34
90.09
DELTA
P
:.H20) (
• 004
.004
.004
.008
.008
.008
.006
.006
.006
.006
.006
.006
DELTA
H
I.H20)
.250
.250
.250
.400
.400
.400
.300
.300
.300
.350
.400
.400
TEMP
IN
(D.F)
44.0
47.0
51.0
48.0
53.0
59.0
52.0
58.0
62.0
52.0
57.0
63.0
TEMP
OUT
(D.F)
45.0
45.0
45.0
46.0
47.0
47.0
48.0
49.0
50.0
50.0
51.0
51.0
TRAIN
VAC
(I»HG)
3.0
4.0
6.0
9.0
9.0
9.5
9.5
11.0
13.5
3.0
3.0
4.0
STACK S.GEL
TEMP TEMP
(D.F) (D.F)
170.0
170.0
170.0
200.0
200.0
205.0 56.0
170.0
160.0
160.0
170.0
185.0 50.0
190.0
PROBE
T DIA
(IN)
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
VEL
(FPM)
250.0
250.0
250.0
350.0
350.0
350.0
300.0
300.0
300.0
300.0
300.0
300.0

-------
      TABLE C-6   (Concluded)



RUN-    11     PATE.- 12-07-75
PORT-
POINT

6
6
6
7
7
7
8
8
8
2
2
2

1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5*00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL

-------
                                       TABLE C-7
                            ORGANIC DATA AND CALCULATED VALUES
                          RUM-    13
 OATK- 12-08-75
 ATMOS  ATMOS  STACK   H?0    PARTIC
 TEMP   PRES    VAC   CONO    WT-PTL
(06.F) (J.HG) (I.H20) (ML)      (MO)
PARTIC  STACK   INIT
WT-TTL   AREA    VOL
 (MO)   (FT2)   (DCF)
PERC PERC PERC  PITOT
 02   C02  CO    TUBF.
 DRY  DRY  DRY   COEF
 40.0   29.35   0.00   52.5-  1013.70   1698.20    ,20  111.14   1.1  22.3  6.7  .850
PORT-
POINT

1
1
1
2
2

1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
112.45
113.52
115.01
116.04
116.76
DELTA
P
I.H20)
.005
.005
.005
.003
.003
DELTA
H
(I.H20)
.250
.200
.300
.100
.050
TEMP
IN
(D.F)
42.0
45.0
50.0
42.0
45.0
TEMP
OUT
(D.F)
45.0
45.0
45.0
44.0
45.0
TRAIN
VAC
(I. HO)
9.0
14.0
5.0
10.0
15.0
STACK S.GEL
TEMP TEMP
(D.F) (D.F)
320.0
325.0
290.0
320.0
330.0
PROBE
T DIA
(IN)
.600
.600
.600
.600
.600

VEL
(FPM)
300.0
300.0
300.0
250.0
250.0

-------
                                             TABLE C-8
                                   ORGANIC DATA AND CALCULATED VALUES
                                 RUN-   14
                                        HATE- 12-08-75
 ATMOS   ATMOS   STACK    H20     PARTIC
 TEMP   PRES     VAC    COND     WT-PTL
(DG.F)  (I.HG)  (I.H20)  (ML)-     (MG)
  PARTIC  STACK  INIT
  WT-TTL   AREA   VOL
   (MG)   (FT2)  (DCF)
        40.0   29.35   0.00  176.0  4911.40  6965.90
                                                                    PERC PERC PERC PITOT
                                                                     02   CO?  CO    TUBE
                                                                     DRY  DRY  DRY   COEF
                                                 .20  116.76  1.1 22.3  6.7  .850
NJ
PORT-
POINT

1
1
2
2
4
4
3
3
5
5
6
6
7
7

1
1
1
1
1
1
1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) 1
118.09
119.36
120.21
120.98
122.15
123.22
124.27
125.27
126.59
127.71
129.27
130.65
132.00
133.17
                      DELTA    DELTA   TEMP   TEMP TRAIN  STACK S.GEL PROBE
                        P        H      IN     OUT  VAC    TEMP  TEMP T DIA
              (DCF)  (I.H20)  (UH20)  (D.F)  (D.F)  (I.HG)  (D.F) (D.F) (IN)
                              .005
                              .005
                              .002
                              .002
                              .003
                              .003
                              .003
                              .002
                              .006
                              .006
                              .004
                              .004
                              .004
                              .004
                               .200
                               .200
                               .100
                               .100
                               .200
                               .200
                               .200
                               .150
                               .250
                               .150
                               .300
                               .300
                               .300
                               .250
43.0
46.0
46.0
47.0
50.0
53.0
45.0
47.0
46.0
48.0
49.0
54.0
52.0
55.0
45.0
46.0
46.0
47.0
48.0
48.0
47.0
47.0
47.0
47.0
47.0
48*0
49.0
50.0
 2.5
 5.0
 7.0
12.0
 4.0
10.0
 4.0
11.0
 8.0
 8.0
 4.0
 9.0
 1.0
 2.0
325. 0
320.0
325.0
330.0
235.0
245.0
200.0
215.0
335.0
335.0
295.0
325.0
300.0
325.0
50.0
50.0
50.0
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
.600
 VEL
(FPM)

300.0
300.0
200.0
200.0
220.0
220.0
200.0
200.0
340.0
340.0
2BO.O
280.0
280.0
280.0

-------
                                   TABLE C-9
                             ORGANIC EMISSION DATA
NAME       DESCRIPTION
        DATE  OF RUN
UNITS      .1.....	  3          5

         12-02-75   12-03-75   12-04-75
DN
TT
PB
PM
VM
TM
VMSTD
VW
VWV
PMOS
MD
PC02
P02
PCO
PN2
MWD
MW
CP
DPS
TS
NP
PST
PS
VS
AS
QS
QA
PERI
MF
MT
1C
CAN
CAO
CAT
CAU
CAW
CAX
EA
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY G6S-STD COND
TOTAL H?0 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL« DRY
PERCENT 02 BY VOL t DRY
PERCENT CO BY VOL » DRY
PERCENT N2 BY VOL» DRY
MOLECULAR *T-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TU6E COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE* DRYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAD-PTLtSTD CN
PART. LOAD-TTL»STD CN
PART. LOAD-PTL,STK CN
PART. LOAD-TTL.STK CN
PARTIC EMIS-PARTIAL
PARTIC EMIS-TOTAL
PERCENT EXCESS AIR
IN
WIN
IN.HG
IN.H20
DCF
DEG.F
DSCF
ML
SCF









IN.H20
DEG.F

IN.HG
IN.HG
FPM
IN2
DSCFM
	 ACFM

MG
MG

GR/DSCF
GR/DSCF
GR/ACF
GR/ACF
LB/HR
LB/HR

.600
30.0
.29.26
.442
11.35
68. 4
11.15
31.0
.1,47
11.6
.884
11.0
9.2
1.9
77.9
30.13
28.72
.850
,007
52.0
6
-0.00
29.26
275a/
11,310^'
19,326*/
21,60l£/
76.7
554.90
646.70
14.20
.76674
.89358
.68577
.79922
127
" 149
67
.600
240.0
..29.31
.506
96.34
75.5
93.53
675.2
32.00
25.5
.745
11.0
9.2
1.9
77.9
30.13
27.04
.850
.008
150.5
48
-0.00
29.31
332
29
42
66
94.0
1574.60
3367.30
53.24
.25926
.55443
.16427
.35129,
.09E/
.20k/
67
.600
160.0
29.31
.539
67.08
79.8
64.61
598.0
2£.35
30.5
.695
15.0
7.3
2.9
76.8
30.69
26.82
.850
.008
158.3
32
-0.00
29.31
353
29
41
71
99.5
2515.50
6815.40
63.09
.59961
1.62455
.34997
.94819
.2l£'
.57k/
42
  a/  Nominal 10-ft (120 in.) diameter stack.
  b/  Per stack; to obtain total for kiln, multiply by 8.
                                      93

-------
                          TABLE C-9  (Continued)
NAME

DN
TT
P8
PM
VM
TM
VMSTD-.
V«
VWV
PMOS ..
MO
PC02
P.02-. . .
PCO
PN2
M.WD -
MW
CP
DPS
TS
NP
PST .
PS
VS
AS
QS
QA
PERI ...
MF
MT
.1C-... -
CAN
CAO
CAT . .
CAU
CAW
CAX .. . .
EA
DESCRIPTION
DATE OF RUN
PROBE T i P -o i A METER 	 -
NET TIME OF RUN
BAROMETRIC PRESSURE
.AV.G ORIFICE.. PRES. .DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL- D&Y..-GAS--STD-CONO 	
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT .MUlSTURE. BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL» DRY
..PERCENT. ...02- BY ..VOL* DRY 	
PERCENT CO BY VOL* DRY
PERCENT N2 BY VOL» DRY
MOLECULAR- KT-.DRY. STK. GAS
MOLECULAR *T-STK GAS
PITOT TUBE COEFFICIENT
AVG STK -VELXJCI-I-Y... HEAD •
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF 	 STACK
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
STACK- AREA
STK FLOWRATE. DRY»STD CN
ACTUAL STACK FLOWRATE
PERCENT -ISOK.INE-TI.C- . .. ...
PARTICULATE teT-PARTIAL
PARTICULATE WT-TOTAL
PERC -iMPlNuER-CAICH- ~~
PART. LOAD-PTL»STD CN
PART. LOAD-TTL»STD CN
.P.AKT..-LOAD.-P~TL-».STK~CN 	
PART. LOAD-TTL»STK CN
PARTIC EMIS-PARTIAL
P. ART-I C. EM.LS---TQ T AJ 	 	 -
PERCENT EXCESS AIR
UNITS

IN
MIN
IN.HG
-IN.H20
DCF
DEG.F
	 DSCF
ML
SCF



. .





IN.H20
DEG.F

. -IN.HG
IN.HG
FPM
- IN2
— A t ' C»
DSCFM
ACFM

MG
MG

GR/DSCF
GR/DSCF
GR/ACF-
GR/ACF
LB/HR
LB/HR ...

7
12-05-75
.600
160.0
29.25
.412
57.24
79,8
55.00
624.7
29.61
35.0
.650
17.2
9.2
4.1
69.5
31.12
26.53
.850
:..... .006
164.8
32
-0.00
29.25
309
29
33
62
-104.6
7996.00
48040.40
.-.-- -83.36
2.23896
13.45180
1.20683
7.25071
.64*
3.85-
64
                                                                   11
                                                     12-06-75   12-07-75
                                                          .600
                                                        105.0
                                                        29.65
                                                          .350
                                                        34.18
                                                          53.3
                                                       -35.00
                                                        316.4
                                                        15.00
                                                          30.0
                                                          .700
                                                          16.1
                                                       - - 6.4	
                                                          1.5
                                                          76.0
                                                        30.83
                                                        26.98
                                                          .850
                                                          .006-
                                                        157.1
                                                            21
                                                        -0.00
                                                        29.65
                                                          293
                                                            29
                                                            35
                                                            59
                                                      	  97-.0 -
                                                      2855.50
                                                      6491.20
                                                      . - 56.4)1-
                                                      1.25636
                                                      2.85599
                                                       .74851 -
                                                      1.70152
                                                           oob/
                                                             K/
                                                            Qcb/..
                                                      -•••  •- .oj—
                                                            39
    .600
   120.0
   29.65
    ,319
   37.53
    54.4
 -  38.35
   370.0
   17.54
  --31.4
    .686
    18.2
	  5,1
     5.5
    71.2
	31.12
   27.00
    .850
    .006
   202.7
      24
	-0.00
   29.65
     300
	29
      33
      60
    99.4
 4777.90
 8821,20
  -45.84.
 1.91649
 3.54201
-1.04336
 1.92630
       a/
     -.99i
      14
_a/  Per stack; to obtain total for kiln, multiply by 8.
b/  Per stack; to obtain total for kiln, multiply by 7.
                                   94

-------
                       TABLE C-9  (Concluded)
NAME       DESCRIPTION

        DATE  OF RUN
UNITS
1.1
14
         12-08-75  12-08-75
ON
TT
PB
PM
VM
TM
VMSTD
VW
VWV
PMOS
MD
PC02
P02
PCO
PN2
MWD
MW
CP
DPS
TS
NP
PST
PS
VS
AS
QS
QA
PERI
MF
MT
1C
CAN
CAO
CAT
CAU
CAW
CAX
EA
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL, DRY
PERCENT 02 BY VOL, DRY
PERCENT CO BY VOL, DRY
PERCENT N2 BY VOL, DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUHE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE, DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAD-PTL,STD CN
PART. LOAD-TTL,STD CN
PART. LOAD-PTL,STK CN
PART. LOAD-TTL,STK CN
PARTIC EMIS-PARTIAL
PARTIC EMIS-TOTAL
PERCENT EXCESS AIR
IN
MIN
IN.HG
IN.H20
DCF
OEG.F
DSCF
ML
SCF









IM.H20
DEG.F

IN.HG
IN.HG
FPM
IN2
DSCFM
ACFM

MG
MG

GR/DSCF
GR/DSCF
GR/ACF
GR/ACF
L8/HR
LB/HR

,600
25.0
29.35
.180
5.62
44.8
5.79
52.5
2.49
30.1
.699
22.3
1*1
6.7
69.9
31.61
27.52
.850
.004
317.0
5
-0.00
29.35
280
29
26
56
89.7
1013.70
1698.20
40.31
2.69585
4.51621
1.26165
2.11358 .
Ma/
• ol—
l.Oll/
-11
.600
70.0
29.35
.207
16.41
48.0
16.80
176.0
8.34
33.2
.668
22.3
1.1
6.7
69.9
31.61
27.10
.850
.004
293.6
14
-0.00
29.35
260
29
2*
52
101.7
4911.40
6965.90
29.49
4.50094
6.38374
2.07511
2.94315
.92^
1.31^
-11
aj  Per stack; to obtain total,  multiply by 1.67.
b/  Per stack; to obtain total for kiln, multiply by 7.
                                 95

-------
                                   TABLE C-10
                              ORGANIC EMISSION DATA
                                (METRIC RESULTS)
NAME       DESCRIPTION

        DATE  OF RUN
UNITS
         12-02-.7S	12-03-75  .12-0.4-J5
ON
TT
PB
PM
VM
TM
VMSTM
VW
VWM
PMOS
MD
PC02
P02
PCO
PN2
MUD
MW
CP
DPS
TSM
NP
PST
PS
VSM
AS
QSM
QAM
PERI
MF
MT
1C
CANM
CAOM
CATM
CAUM
CAWM
CAXM
EA
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H2C COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL, DRY
PERCENT 02 BY VOL, DRY
PERCENT CO BY VOL, DRY
PERCENT N2 BY VOL, DRY
MOLECULAR KT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLO*RATE, DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAD-PTL,STD CN
PART. LOAD-TTL>STD CN
PART. LOAD-PTUSTK CN
PART. LOAD-TTL,STK CN
PARTIC EMIS-PARTIAL
PARTIC EMIS-TOTAL
PERCENT EXCESS AIR
IN
MJ.N 	
IN.HG
IN.H20
DCF
DEG.F
NCM
.. .ML ...
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
"M3/MIN "~

KG
MG

MG/NM3
"MG/NM3
MG/M3
MG/M3
KG/HR
KG/HR
•- 	 - -
.600
... 3.0.0 	
29.26
.442
.. ...11,35
68.4
.32
	 3U.Q._
.04
11.6
.884
11.0
9.2
1.9
77.9
30.13
28.72
.850
.007
11.1
6
-0.00
29.26
83.8 .
11,310£/
5 47 a/
612a/™
76.7
554.90
646.70
14.20
1754.55
2044.82
1569.28
1828.89
™ 58
67
67
.600
240.0
29.31
.506
96.34
75.5
2.65
6J5,2.
.91
25.5
.745
11.0
9.2
1.9
77.9
30.13
27.04
.850
.008
65.8
48
-0.00
29.31
101.2
29
1.2
1.9
94.0
1574.60
3367.30
53.24
593.28
1268.73
375.90
803.87,
.042^
.09Lk/
67
.600
160.0
29.31
.539
67.08
79.8
1.03
596.0
.80
30.5
,6.95
15.0
7.3
2.9
74.8"
30.69
26.82
.850
.008
70.1
32
-0.00
29.31
107.7
29
1.2
2.0
99.5
2515.50
6615.40
63.09
1372.10
3717.52
800.85
2169.79
,096k/
.260k/
42
a./  Nominal  10-ft (120 in.)  diameter stack.
b/  Per stack;  to obtain total  for kiln, multiply by 8,
                                      96

-------
                              TABLE C-10  (Continued)
NAME

DN
TT
PS
PM
VM
TM ..
VMSTM
Vw
VWM
PMOS
MO
PC02
P02
PCO
PN2
MWO
MW
CP 	
DPS
TSM
.NP .. .
PST
PS
.VSM ... .
AS
QSM
QAM . .
PERI
MF
..MT
1C
CANM
CAOM
CATM
CAUM
CArfM..
CAXM
EA
-DESCfilPT-ION 	 -. - . ...
DATE OF RUM
PROBE TIP DIAMETER
NET TIw.F. OF RUN
BAROMETRIC. PRESSURE 	
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
. _AV.G- GAS-METER -TEMP _ 	 ___
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H2G .VAPQP-STD- COND-
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT..C02 BY-VOL, -DRY-
PERCENT 02 BY VOL» DRY
PERCENT CO BY VOL» DRY
PERCENT .N2- 8Y-VOL-* DRY-
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
....P1TO-T-..TUBE.-COEF.F4C1ENT.-.'—
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
.. .NET SAMPLING. PO-INTS 	 	
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
--AV.G -STACK... &AS-VE-L-OCITY 	
STACK A*EA
STK FLOtfRATEt DRY,STD CN
UNITS

IN
MIN
IN.HG
IN.H20
DCF
-DEG,F -
NCM
ML
NM3





—


. 	 	
IM.H20
DEG.C
..._.-. - .
IN.HG
IN.HG
.-_M/M.IN
IN2
NM3/MIN
. ACTUAL. 5T.ACK~.F.LO.»iRAT£ 	 M3/MIN -
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PAHTICULATE- WT-TOTAL - -
PERC IMPINGER CATCH
PART. LOAD-PTL»STD CN
PART.. -LOADf.TTUSTD.-CN 	
PART. LOAD-PTL»STK CN
PART. LOAO-TTL»STK CN
.PARTIC. . EMI S -PARTIAL 	
PARTIC EMIS-TOTAL
PERCENT EXCESS AIR

MG
	 MG- -

MG/NM3
-MG/NM-3 -
MG/M3
MG/M3
_K.G/HR. . .

-------
                      TABLE C-10  (Concluded)
NAME       DESCRIPTION

        DATE  OF  RUN
UNITS
13
14
         12-58-75  .12-08-75.
DN
TT
PB
PM
VM
TM
VMSTH
VW
VWM
PMOS
MD
PC02
P02
PCO
PN2
MHD
MW
CP
DPS
TSH
NP
PST
PS
VSM
AS
QSM
QAM
PERI
MF
MT
1C
CANM
CAOM
CATM
CAUM
CAHM
CAXM
EA
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STO COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL» DRY
PERCENT 02 BY VOL, DRY
PERCENT CO BY VOL» DRY
PERCENT N2 BY VOLt DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLO*RATE, DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PARTICULATE WT-PARTIAL
PARTICULATE WT-TOTAL
PERC IMPINGER CATCH
PART. LOAD-PTL»STD CN
PART. LOAD-TTL.STD CN
PART. LOAD-PTL*STK CN
PART. LOAD-TTL»STK CN
PARTIC EMIS-PARTIAL
PARTIC EMIS-TOTAL
PERCENT EXCESS AIR
IN
KIN
IN.HG
IN.H20
DCF
DEG.F
NCM
ML
NM3
IN.H20
DEG.C
IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
M3/MIN
MG
MG
MG/NM3
MG/NM3
M5/M3
MG/M3
KG/HR
KG/HR
.600
	 	 ._25.»0
29.35
• 180
5.62..
•+4.6
.16
52.5
.07
30.1
_ ,699
22,3
1.1
6.7
69.9
31.61
27.52
.850
,004
158.3
5
-0.00
29.35
85.4
29
.7
1,6
89.7
1013.70
1698.20
40.31
6169.01
10334.63
2887.09
4836.60
.275*/
.460i/
	 -_11 .
.600
„... 70.0
29.35
.207
16.41
48.0
.48
176.0
.24
33.2
,668
22.3
1.1
6.7
69.9
31.61
27.10
.850
.004
145.3
14
-0.00
29.35
79.3
29
.7
1,5
101.7
4911.40
6965.90
29.49
10299.68
14608.16
4748.56
6734.94
.42 O^/
.595^
-11
a/  Per stack; to obtain total, multiply by 1.67.
b/  Per stack; to obtain total for kiln, multiply by 7.
                                98

-------
                                                      TABLE C-ll
                                             SUMMARY OF RESULTS  (ORGANIC)
vo
NAME

VMSTD
PMOS
TS
OS
QA
PERI
DESCRIPTION
DATE OF RUN
VOL DRY GAS-STD COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE, DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
UNITS

OSCF

DEG.F
DSCFM
ACFM

I
12-02-75
11.15
11.6
52,0
ii,3io*/
21,601*'
76.7
3
12-03-75
93.53
25.5
150.5
42
66
94.0
5
12-04-75
64.61
30,5
158.3
41
71
99.5
PARTICULATES — PARTIAL CATCH
MF
CAN
CAT
CAW
PARTI
MT
CAO
CAU
CAX
1C
PARTICULATE WT-PARTIAU
PART. LOAD-PTL.STD CN
PART. LOAD-PTL.STK CN
PARTIC EMIS-PARTIAL
CULATES — TOTAL CATCH
PARTICULATE WT-TOTAL
PART. LOAD-TTL,STD CN
PART. LOAD-TTL:,STK CN
PARTIC EMIS-TOTAL
PERC IMPINGER CATCH
MO
OR/DSCF
GR/ACF
LB/HR

MG
GR/DSCF
GR/ACF
LB/HR

554.90
.76674
.68577
180

646.70
.89358
.79922
219
14.20
1574.60
.25926
.16427 .
.09^/

3367.30
.55443
.35129
.2(£'
53.24
2515,50
,59961
.34997
.21^

6815,40
1,62455
.94819
.57^
63.09
                 aj  Nominal 10-ft (120 in.) diameter stack.
                 b/  Per stack; to obtain total for kiln, multiply by 8.

-------
                                                TABLE C-ll  (Continued)
o
o
NAME

VMSTD
PMOS
TS
QS
OA
PERI
PARTI
MF
CAN
CAT
CAW
PARTI
MT
CAO
CAU
CAX
1C
DESCRIPTION
DATE OF HUM
VOL DRY GAS-STD COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATEt DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
CULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAO-PTL«STD CN
PART. LOAD-PTL,STK CN
PARTIC EMIS-PARTIAL .
CULATES — TOTAL CATCH
PARTICULATE WT-TOTAL
PART. LOAD-TTL,STD CN
PART. LOAD-TTL.STK CN
PARTIC EMIS-TOTAL
PERC IMPINGER CATCH
UNITS

DSCF

DEG.F
DSCFM
ACFM


MG
GR/DSCF
GR/ACF
LB/HR

MG
GR/DSCF
GR/ACF
l.B/HR

7
12-05-75
55.00
35.0
164.8
33
62
104.6

7996.00
2.23896
1.20683
.64£/

48040.40
13.45180
7.25071
3.85*'
03.36
9
12-06-75
35.00
30.0
157.1
35
59
97.0

2855.50
1.25636
.74851
.38k/

6491.20
2.85599
1.70152
.85k/
56.01
11
12-07-75
38.35
31.4
202.7
33
60
99.4

4777.90
1.91849
1.04336 ,
.54£/

8821.20
3.54201
1.92630 ,
.99^
45.84
                aj  Per stack; to obtain total for kiln, multiply by 8.

                b_/  Per stack; to obtain total for kiln, multiply by 7.

-------
                          TABLE C-ll  (Concluded)
NAME       DESCRIPTION

        DATE  OF RUN
UNITS
VMSTD
PMOS
TS
QS
QA
PERI
VOL DRY G/VS-STD COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE* DRY»STD CM
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
DSCF

DEG.F
DSCFM
ACFM

PARTICULATES — PARTIAL CATCH
MF
CAN
CAT
CAW
PARTI
MT
CAO
CAU
CAX
1C
PARTICULATE WT-PARTIAL
PART. LOAO-PTL.STD CN
PART. LOAO-PTL.STK CN
PARTIC EMIS-PARTIAL
CULATES — TOTAL CATCH
PARTICULATE WT-TOTAL
PART. LOAD-TTL»STD CN
PART. LOAD-TTL»STK CN
PARTIC EMIS-TOTAL
PERC IMPINGER CATCH
MG
GR/DSCF
GR/ACF
LB/HR

MO
GR/DSCF
GR/ACF
LB/HR

13
12-08-75
5.79
30.1
317.0
26
56
89.7
1013.70
2.69585
1.26165
.6l£/
1698.20
4.51621
2.11358 ,
14
12-08-75
16.80
33.2
293.6
24
5?
101.7
4911.40
4.50094
2.07511 ,
.92k/
6965.90
6.38374
2.94315 ,
                                                   40.31
                        29.49
aj  Per stack; to obtain total, multiply by 1.67.
b_/  Per stack; to obtain total  for kiln, multiply by 7,

-------
                                                TABLE C-12
                                  SUMMARY OF RESULTS—METRIC UNITS (ORGANIC)
o
ro
              NAME       DESCRIPTION

                      DATE OF  RUN
UNITS
VMSTM VOL DRY GAS-STD COND
PMOS
TSM
QSM
QAM
PERI
EA
PART
MF
CANM
CATM
CAWM
PART
MT
CAOM
CAUM
CAXM
1C
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE* DRY,STD CN
ACTUAL STACK FLOWRATK
PERCENT ISOKINETIC
PERCENT EXCESS AIR
ICULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAO-PTL,STD CN
PART. LOAD-PTLtSTK CN
PARTIC F:MIS-PARTIAL
ICULATES — TOTAL CATCH
PARTICULATE WT-TOTAL
PART. LOAD-TTL.STD CN
PART. LOAD-TTLtSTK CN
PARTIC EMIS-TOTAL
PERC IMPINGER CATCH
NCM

DEG.C
NM3/MIN
M3/MIN



MG
MO/NM3
MG/M3
KG/HR

MG
MG/NM3
MG/M3
KG/HR

  1           3          5

12-02-75   12-03-75   12-04-75
.316
11.6
11.1 .
547£/
612^'
76.7
67
2.649
25.5
65.fi
1.2
1.9
94.0
67
1.029
30.5
70.1
1.2
2.0
99.5
42
                                                             554.90
                                                            1754.55
                                                            1569.28
                                                                  58
                     1574.60    2515,50
                      593.28    1372.10
                      375.90     800.85
                         .042k/      .096k/
MG
MG/NM3
MG/M3
KG/HR

646.70
2044.82
1828.89
67
14.20
3367.30
1268.73
803.87
.09lk/
53.24
6815.40
3717.52
2169.79
• £. O^J—
63.09
               a/  Nominal  10-ft (120 in.) diameter stack.
               b/  Per stack; to obtain total  for kiln, multiply by 8.

-------
                             TABLE G-12  (Continued)
NAME       DESCRIPTION

        DATE OF RUM
UNITS        7          9         11

         12-05-75   12-06-75   12-07-75
VMSTM VOL DRY GAS-STD COND
PMOS
TSM
QSM
QAM
PERI
EA
PART
MF
CANM
CATM
CAWM
PART
MT
CAOM
CAUM
CAXM
1C
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATEt ORY«STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PERCENT EXCESS AIR
ICULATE.S — PARTIAL CATCH
PARTICULAR WT-PARTIAL
PART. LOAD-PTL,STD CN
PART. LOAO-PTL.STK CN
PARTIC EMIS-PARTIAL
ICULATES — TOTAL CATCH
PARTICULAR WT-TOTAL
PART, LOAD-TTL»STD CN
PART. LOAU-TTL.STK CN
PARTIC EMIS-TOTAL
PERC IMPINGER CATCH
NCM

DEG.C
NM3/MIN
M3/MIN



MG
MG/NM3
MG/M3
KG/HR

MG
MG/NM3
MG/M3
KG/HR

1.557
35.0
73.8
.9
1.8
104.6
64

7996.00
5123.51
2761.64
.29Q£

48040.40
30782.30
16592.09
1.744*'
83.36
.991
30.0
69.5
1.0
1.7
97.0
39

2855.50
2874.98
1712.83
.1702/

6491.20
6535.49
3893.66
.387^
56.01
                                                                    4777.90
                                                                    4390.16
                                                                    2387.56
                                                                       .243-'
                                                                    8821.20
                                                                    8105.33
                                                                    4409.03
                                                                      45.84
aj  Per stack;  to obtain  total for kiln, multiply by  8.
b/  Per stack;  to obtain  total for kiln, multiply by  7.

-------
                       TABLE C-12  (Concluded)
NAME
VMSTM
PMOS
TSM
QSM
QAM
PERI
EA
   DESCRIPTION

DATE OF RUN
                           UNITS
                             NCM
VOL DRY GAS-STD CONO
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE      DEG.C
STK FLOWRATE, DRYtSTD  CN  NM3/MIN
ACTUAL STACK FLOWRATE     M3/MIN
PERCENT ISOKINETIC
PERCENT EXCESS AIR
PARTICULATES — PARTIAL  CATCH

MF     PARTICULATE WT-PARTIAL
CANM   PART. LOAD-PTLfSTD  CN
CATM   PART. LOAD-PTL»STK  CN
CAWM   PARTIC FMIS-PARTIAL

PARTICULATES — TOTAL  CATCH

MT     PARTICULATE WT-TOTAL
CAOM   PART. LOAD-TTL«STD  CN
CAUM   PART. LOAD-TTL.STK  CN
CAXM   PARTIC EMIS-TOTAL
1C     PERC IMPINGF.R CATCH
                              MO
                          MO/NM3
                           MG/M3
                           KG/HR
   13        14

12-08-75  12-08-75
,164
30.1
158.3
.7
1.6
89.7
-11
.476
33.2
145.3
.7
1.5
101.7
-11
                                    1013.70   4911.40
                                    6169.01   10299.68
                                    2887.09   4748.56
                                       .275£/
MG
MG/NM3
MG/M3
KG/HR
1698.20
10334.63
4836.60 .
.460*/
40.31
6965.90
14608.16
6734.94
.595^'
29.49
aj  Per stack; to obtain total, multiply by 1,67.
b_/  Per stack; to obtain total for kiln, multiply  by 7.

-------
                APPENDIX D
RESULTS OF ANALYSIS - COMPUTER COMPUTATIONS
      (POLYCYCLIG ORGANIC MATERIALS)
                    105

-------
                                           TABLE D-l





                        BENZ[V]PHENANTHRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG.F
40.0
)

PORT-
POINT

1
2
4
3
5
6
7
8

1
1
1
1
1
1
1
1
ATMOS
PRES
(I.HG)
29.31
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
838.98
840.69
842.82
845.03
847.27
849.49
851.22
853.23
RUN- 2
H?0 PARTIC
COND WT-PTL
(ML)
109.8
DELTA
P
I.H20) i
.005
.006
.009
.009
.011
.011
.004
.008
(MG)
15.40*/
DELTA
H
1I.H20) (
.270
.400
.650
.700
.700
.650
.450
.550
DATE- 12-03-75
PARTIC STACK
WT-TTL AREA
(MG) (
15
TEMP
IN
D.F)
43.0
49.0
53.0
58.0
62.0
64.0
65.0
65.0
.40£/
TEMP
OUT
(D.F)
43.0
49.0
53.0
60.0
62.0
64.0
66.0
65.0
FT?)
.20
TRAIN
VAC
(I.HG)
8.5
5.0
5.0
6.0
9.0
7.0
12.0
12.0
INIT
VOL
(DCF)
837.66
STACK
TEMP
(D.F)
140.0
145.0
130.0
140.0
160.0
155.0
165.0
165.0
PERC PERC PFRC PITOT
02 CO? CO TUBE
DRY DRY DRY COEF
9.2 11.0 1
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
.600
.600
.600
.600
.9 .850

VEL
(FPM)
260.0
300.0
350.0
350.0
400.0
400.0
250.0
350.0
il   x  10-3.

-------
                                      TABLE D-2


                      BENZ[V]PHENANTHRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG.F)
50.0
PORT-
POINT

1
2
4
3
5
6
7
8

1
1
1
1
1
1
1
1
ATMOS
PRES
(I.HG)
29.31
SAMP
TIME
( MI N )
5,00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (]
854.97
057.01
859.01
860.85
863.15
865.45
867.35
869.71
RUN- 4 DATE- 12-04-75
H?0 PARTIC PARTIC STACK
COND WT-PTL WT-TTL AREA
(ML) (MG) (MG) (FT2)
134.4 3.402/ 23.40£/ .20
DELTA DELTA TEMP TEMP TRAIN
p H IN OUT VAC
t.H20) (
.004
.008
.008
.007
.011
.011
.006
.011
I.H20)
.500
.600
.550
.500
.700
.700
.600
.700
(D.F)
64.0
58.0
61.0
64.0
68.0
72.0
73.0
75.0
(D.F)
66.0
60.0
61.0
64.0
68.0
72.0
73.0
75.0
(I.HG)
5.0
7.5
5.5
5.0
12.0
9.0
5.0
13.0
INIT
VOL
(DCF)
853.51
STACK
TEMP
(D.F)
150.0
145.0
160.0
160.0
165.0
150.0
160.0
155.0
                                                               PERC  PERC PERC  PITOT
                                                                02    C02  CO    TUBF
                                                                DRY   DRY  DRY   COEF

                                                                7.3  15.0  2.9   .850
                                                               S.GEL PROBE
                                                                 TEMP T
                                                                (D.F) (
niA
IN)
.600
.600
.600
.600
.600
.600
.600
.600
VEL
CFPM)
250.0
350.0
350.0
320.0
400.0
400.0
300.0
400.0
a/


-------
o
00
                                                        TABLE D-3



                                     BENZ|V]PHENANTHRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG.F)
50.0
PORT-
POINT

1 1
2 1
4 1
3 1
5 1
6 1
7 1
8 1
ATMOS
PRES
(I.HG)
29.25
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
-0.00
METER
VOL.
(DCF) (
871.25
872.97
874.84
076.42
878.15
879.83
882.05
883.70
RUN- 6
H20 PARTIC
CONO WT-PTL
( ML )
154.8
DELTA
P
I.H20)
.004
.006
.006
.004
.006
.006
.010
.006
(MG)
ll.OQi/
DELTA
H
(I.H20) (
.300
.350
.450
.300
.400
.400
.700
.400
DATE- 12-05-75
PARTIC STACK INIT
WT-TTL AREA VOL
(MG) 1
11
TEMP
IN
D.F)
68.0
67.0
67.0
69.0
66.0
68.0
70.0
70.0
.00£/
TEMP
OUT
(D.F)
70.0
67.0
67.0
69.0
67.0
68.0
70.0
70.0
[FT?)
.20
TRAIN
VAC
(I.HG)
5.0
5.0
5.0
5.0
7.0
B.O
10.5
7.0
(DCF)
869.81
STACK
TEMP
(D.F)
155.0
155.0
150.0
160.0
160.0
165.0
180.0
185.0
PERC PERC PERC PITOT
02 C02 CO TUBE
DRY DRY DRY COEF
9.2 17.2 4
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
70.0 .600
.600
.600
.600
.600
.600
.600
.600
.1 .850

VEL
(FPM)
250.0
300.0
300.0
250.0
300.0
300.0
400.0
300.0
           »7  x 10-3.

-------
                                       TABLE D-4


                       BENZ[c~]PHENANTHRENE DATA AND CALCULATED VALUES
 ATMOS  ATMOS  STACK
 TEMP   PRES    VAC
(DG.F) (I.HG) (I.H20)  (ML)
RUN-
H20
OND
ML)
8
PARTIC
WT-PTL
(MG)
DATE-
PARTIC
WT-TTL
(MG)
12-06-75
STACK INIT
AREA VOL
(FT2) (DCF)
 40.0
29.65   0.00   96.1
0.002.'
                                    a/
                                         19.80E'
                                                       PERC PERC PERC PITOT
                                                        02   C02   CO    TUBE
                                                        DRY  DRY   DRY  COEF
.20  883.70  6.4  16.1   1.5  .850
 PORT-  SAMP  METER   OELTA    DELTA  TEMP  TEMP  TRAIN  STACK 5.GEL PROBE
 POINT  TIME   VOL       P        H     IN    OUT   VAC    TEMP  TEMP T  DIA    VEL
       (MIN)  (OCF)  (I.H20)  (I.H20) (D.F)  (D.F)  (I.HG)  (D.F) (D.F) (IN)    (FPM)

                                                                       .600   250.0
                                                                       .600   300.0
                                                                       .600   300.0
                                                                70.0   .600   250.0
                                                                       .600   300.0
                                                                       *600   300.0
                                                                       .600   300.0
  a/  Not detectable.
4
3
5
6
7
8
1
1
1
1
1
1
1
1
5.00
5.00
5.00
5.00
5.00
5.00
5.00
885.07
886.77
888.41
889.80
891.43
893.04
894.69
.004
.006
.006
.004
.006
.006
.006
.250
.400
.400
.250
.400
.400
.400
44.0
42.0
43.0
44.0
44.0
49.0
50.0
46.0
42.0
43.0
44.0
44.0
49.0
50.0
4.0
4.0
4.0
6.0
5.0
9.0
9.0
150.0
140.0
155.0
145.0
160.0
175.0
160.0
  b/  x 10
         -3

-------
                                            TABLE D-5

                         BENZ[£]PHENANTHRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG.F)
40.0
PORT-
POINT

1 1
4 1
3 1
5 1
6 1
7 1
8 1
2 1
ATMOS
PRES
(I.HG)
29.65
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5*00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
896.12
898.14
899.48
901.06
902.40
903.95
905.49
906.78
RUM- 1 0
H20 PARTIC
COND
(ML)
168.0
DELTA
P
I.H20)
.004
.010
.004
.006
.004
• 006
.005
.005
WT-PTL
(MG)
o.oo^/
DELTA
H
(I.HPO) (
.250
.650
.250
.300
.250
.300
.300
.200
HATE- 12-07-75
PARTIC STACK
WT-TTL
(MG
10.3
TEMP
IN
D.F) (
42.0
41.0
41.0
42.0
44.0
46.0
48.0
49.0
)
;ok/
TEMP
OUT
D.F)
45.0
41.0
41.0
42.0
44.0
46.0
48.0
49.0
AREA
(FT2)
.20
TRAIN
VAC
(I.HG)
5.0
11.0
7.0
7.0
7.0
8.0
8.0
8.0
INIT
VOL
(DCF)
894.80
STACK
TEMP
(D.F)
180.0
205.0
165.0
175.0
175.0
185.0
215.0
335.0
PERC PERC PFRC PITOT
02
DRY
5.1 1
S.GEL
TEMP
(D.F)


50.0
60.0


70.0

C02
DRY
8.2
PROBE
T OIA
(IN)
.600
.600
.600
.600
.600
.600
.600
.600
CO TUBE
DRY COEF
5.5 .850

VEL
(FPM)
250.0
400.0
250.0
300.0
250.0
300.0
300.0
300.0
a/  Not detectable.
b/  x 10-3.

-------
                                            TABLE D-6

                         BENZ[V]PHENANTHRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(06. F)
40.0
PORT-
POINT

1 1
2 1
4 1
3 1
5 1
6 1
7 1
ATMOS
PRES
(I.HG)
29. 3S
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
909.38
910.51
911.59
912.73
913.88
915.17
916.16
RUN- 12 DATE- 12-08-75
H20 PARTIC PARTIC STACK
COND
(Ml.)
83.0
OELTA
P
I.H20)
.005
.003
.003
.003
.004
.004
.003
WT-PTL WT-TTL
(MG)
0.0*
DELTA
H
(I.H20)
.250
.200
.200
.200
.150
.200
.150
(MG)
*/ 27
TEMP
IN
(D.F)
51.0
46.0
42.0
44.0
40.0
41.0
45.0
.3 ok/
TEMP
OUT
(D.F)
54.0
46.0
43.0
44.0
40.0
41.0
42.0
AREA
(FT2)
.20
TRAIN
VAC
(I.HG)
5.0
10.0
4.0
6.0
10.0
4.0
10.0
INIT
VOL
(DCF)
908.17
STACK
TEMP
(D.F)
360.0
330.0
220.0
170.0
230.0
190.0
310.0
PERC PERC PERC PITOT
02 C02
DRY DRY
1.1 22.3
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
.600
50.0 .600
.600
.600
CO TUBE
DRY COEF
6.7 .850

VEL
(FPM)
300.0
250.0
220.0
220.0
240.0
250.0
220.0
a/  Not detectable.
b/  x ID"3.

-------
                                    TABLE D-7
                        BENZ[c]FHENANTHRENE EMISSION DATA
NAME

ON
TT
PB
PM
VM
TM
VMSTD
VW
vwv
PMOS
MO
pco2
P02
PCO
PN2
MWD
MW
CP
DPS
TS
NP
PST
PS
VS
AS
OS
QA
PERI
MF
MT
1C
CAN
CAO
CAT
CAU
CAW
CAX
EA
DESCRIPTION
DATE OF RUN
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRF.S DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL» DRY
PERCENT 02 BY VOL » DRY
PERCENT CO PY VOL* DRY
PERCENT N2 BY VOLt DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUflE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE* DRYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT 1SOKINETIC a/
PARTICULATF WT-PARTIAL"
PARTICULATE WT-TOTAL-'
PERC IMPINGER CATCH a/
PART. LOAD-PTL«STD CN~/
PART. LOAD-TTL»STD CN",
PART. LOAO-PTL»STK CN~/
PART. LOAD-TTL,STK CN~
PARTIC EMIS-PARTIAL-7
PARTIC EMIS-TOTA.L-7
PERCENT EXCESS AIR
UNITS

IN
MIN
IN.HG
IN.H20
DCF
DEG.F
DSCF
ML
SCF









IN.H20
DEG.F

IN.HG
IN.HG
FPM
IN?
DSCFM
ACFM

MG
MG

GR/DSCF
GR/DSCF
GR/ACF
GR/ACF
L8/HR
LB/HR

2
12-03-75
,600
40.0
29.31
.546
15.57
57.6
15.64
109.8
5.20
25.0
.750
11.0
9.2
1.9
77.9
30.13
27.10
.850
.006
150.0
8
-0.00
29.31
333
29
42
67
93.5
15,40
15,40
0.00
.01516
.01516
.00968
.00968
.00552^.
.00552-'
67
4
12-04-75
.600
40.0
29.31
.606
16.20
67.1
15.9R
134.4
6.37
28.5
.715
15.0
7.3
2.9
74.8
30,69
27.07
.850
.008
155.6
8
-0,00
29,31
346
29
4?
6"
97.1
3.40
23.40
85.47
.0032P
.02255
.00198
.01360
.00117^/
.00807^
4?
6
12-05-75
.600
40.0
29,25
.412
13.89
68.3
13.64
154.8
7.34
35.0
.650
17.2
Q.2
4,1
69.5
31.12
26.53
.850
.006
163.H
8
-0,00
29.25
300
?9
32
60
106.8
11.00
11.00
0.00
.01242
.01242
.00671
.00671
.00345^.7
.003452/
64
a/
b/  Per stack; to obtain total for kiln, multiply by 8.
                                       112

-------
NAME
ON
TT
PR
PM
VM
TM
VMSTO
VW
VWV
PMOS
MD
PC02
P02
PCO
PN2
HWD
MW
CP
DPS
TS
NP
PST
PS
VS
AS
QS
OA
PERI
MF
MT
1C
CAN
CAO
CAT
CAU
CAW
CAX
EA
DESCRIPTION
       DATE OF RUN
                          TABLE D-7  (Concluded)
                           UNITS
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL HiiO VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 RY VOL* DRY
PERCENT 02 BY VOL» DRY
PERCENT CO BY VOLt DRY
PERCENT N2 BY VOL. DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
MET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE. ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE, DRY,STD CN
ACTUAL STACK FLOtfRATE
PERCENT ISOKINETIC     /
PARTICULATE WT-PARTIAL~
PARTICULATE WT-TOTAL-7
PERC IMPINGER CATCH  fl/
      LOAD-PTL.STD
      LOAD-TTL.STD
      LOAD-PTL.STK
                           IN
                          MIN
                        IN.HG
                       IN.H20
                          DCF
                        DEG.F
                        DSCF
                           ML
                          SCF
PART.
PART.
PART.
PART.
                   CNI/
      LOAD-TTL.STK CN~
PARTIC F.MIS-PARTI;*'a/
PARTIC EMIS-TOTAL-
PERCENT EXCESS AIR
                       IN.H20
                        DEG.F

                        IN.HG
                        IN.HG
                          FPM
                          IN2
                        DSCFM
                         ACFM

                           MG
                           MG

                      GR/OSCF
                      GR/DSCF
                       GR/ACF
                       GR/ACF
                        LB/HR
                        LB/HR
e
12-06-75
.600
35.0
29.65
.357
10.99
45.3
11.43
96.1
4.56
?8.5
.715
16.1
6.4
1.5
76.0
30.fl3
27.18
.850
.006
155.0
7
-0.00
29.65
286
29
35
57
9S.O
0.00
19.80
100.00
0.00000
.02667
0.00000
.01629
0.00000
,00798k/
39
10
12-07-75
.600
40.0
29.65
.312
11.98
44.3
12.49
160.0
7.96
38.9
.611
18.2
5.1
5.5
71.2
31.12
26.01
.850
.oos
204.4
a
-0.00
29.65
294
29
2a
59
111.8
0.00
10.30
100.00
0.00000
.01270
0.00000
.00613
0.00000
,00309£/
14
12
12-08-75
.600
35.0
29. 3S
.193
7.99
44.2
8.24
83.0
3.93
32.3
.677
22.3
1.1
6.7
69.9
31.61
27.21
.850
.003
258.6
7
-0.00
29.35
243
29
24
49
100.5
0.00
27.30
100.00
0.00000
.05101
0.00000
.02498
0.00000
.01040k/
-11
 a/  x 10-3.
 b/  Per stack; to obtain total for kiln, multiply by 7.
 c/  Per stack; to obtain total for kiln, multiply by 8.
                                  113

-------
                                      TABLE  D-8

                 BENZ[_c]PHENANTHRENE  EMISSION DATA (METRIC RESULTS)
NAME

ON
TT
PB
PM
VM
TM
VMSTM
VW
VWM
PMOS
MO
pco2
P02
PCO
PN2
MWD
MW
CP
DPS
TSM
NP
PST
PS
VSM
AS
QSM
QAM
PERI
MF
MT
1C
CANM
CAOM
CATM
CAUM
CAWM
CAXM
EA
DESCRIPTION
DATE OF HUN
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL. DRY
PERCENT 02 PY VOL. DRY
PERCENT CO BY VOL» DRY
PERCENT N2 BY VOL» DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
AVG STACK GAS VELOCITY
STACK AHEA
STK FLOwRATEt DRY»STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC ,
PARTICULATE WT-PARTIAL-
PARTICULATE WT-TOTAL-
PERC IMPINGER CATCH a/
PART. LOAD-PTL,STD CN-/
PART. LOAD-TTL.STD CN~,
PART. LOAD-PTL»STK CNf,
PART. LOAD-TTLtSTK CN-
PARTIC EMIS-PARTIAL-
PARTIC EMIS-TOTAL-
PEPCENT EXCESS AIR
UNITS

IN
MIN
IN.HG
IN.H20
DCF
HF.G.F
NCM
ML
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
M3/MIN

MG
MR

MG/NM3
MG/NM3
MG/M3
MG/M3
KG/HR
KG/HR

2
12-03-75
.600
A 0.0
29.31
.546
15.57
57.6
.44
109.8
.15
25.0
.750
11.0
9.2
1.9
77.9
30.13
27.10
.850
.008
65.5
8
-0.00
29.31
101.4
29
1.2
1.9
93.5
15.40
15.40
0.00
34.70
34.70
22.16
22.16
,00250k/
.0025 Ok/
67
4
12-04-75
.600
40.0
29.31
.606
16.20
67.1
.45
134.4
.IB
28.5
.715
15.0
7.3
2.9
74.8
30.69
27.07
.850
.008
68.7
8
-0.00
29.31
105.6
29
1.2
2.0
97.1
3.40
23.40
85.47
7.50
51.60
4.52
31.12
.00053J1/
.00366k'
4?
6
12-05-75
.600
40.0
29.25
.412
13.89
68.3
.39
154.8
.21
35.0
,650
17.2
9.2
4.1
69.5
31.12
26.53
.850
.006
73.2
8
-0.00
29.25
01.5
29
.9
1.7
106.8
11.00
11.00
0.00
28.43
28.43
15.35
15.35
.00157k/
.00157k/
64
a/  x 10-3.
b/  Per stack; to obtain total for kiln, multiply by 8.
                                        114

-------
                             TABLE D-8  (Concluded)
NAME       DESCRIPTION

        DATE OF  RUN
UNITS       8           10          12

         12-06-75  12-07-75   12-08-75
ON
TT
PB
PM
VM
TM
VMSTM
VW
VWM
PMOS
MD
PC02
P02
PCO
PN2
MWD
MW
CP
DPS
TSM
NP
PST
PS
VSM
AS
OSM
QAM
PERI
MF
MT
1C
CANM
CAOM
CATM
CAUM
CAWM
CAXM
EA
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H?0 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOLf DRY
PERCENT 0?. BY VOL, DRY
PERCENT CO BY VOL. DRY
PERCENT N2 OY VOL» DRY
MOLECULAR WT-DRY STK GAS
MOLECULAR WT-STK GAS
PITOT TUUE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE. ABSOLUTE
AVG STACK GAS VELOCITY
STACK AREA
STK FLOWRATE* DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKIMETIC ,
PARTICULATE WT-PARTIAIF
PARTICULATE WT-TOTAL-7
PERC IMPINGER CATCH ,
PART. LOAD-PTLfSTD CN-/
PART. LOAD-TTL.STD CN-/
PART. LOAD-PTLtSTK CN~/
PART. LOAD-TTL»STK CN~
PARTIC EMIS-PARTIALr
PARTIC tMIS-TOTAL^'
PERCENT EXCESS AIR
IN
MIN
IN.HG
IN.H20
DCF
OEG.F
NCM
ML
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MTN
M3/MIN
MG
MG
MG/NM3
MG/NM3
MG/M3
MG/M3
KG/HR
KG/HR

.600
35.0
29.65
.357
10.99
45.3
.32
96.1
.13
28.5
.715
16.1
6.4
1.5
76.0
30.83
27.18
.850
.006
68.3
7
-0.00
29.65
87.1
29
1.0
1.6
95.0
0.00
19.80
100.00
0.00
61.03
0.00
37.27
0.00000
.00362^
39
.600
40.0
29.65
.312
11.98
44.3
.35
168.0
.23
38.9
.611
18.2
5.1
5.5
71.2
31.12
26.01
.850
.005
95.8
8
-0.00
29.65
89.6
29
.8
1.7
111.8
0.00
10.30
100.00
0.00
29.07
0.00
14.03
0.00000
.00140£/
14
.600
35.0
29,35
.193
7.99
44.2
.23
83.0
.11
32.3
.677
22.3
1.1
6.7
69.9
31,61
27.21
.850
.003
125.9
7
-0.00
29.35
74.0
29
.7
1.4
100.5
0.00
27.30
100.00
0.00
116.72
0.00
57.16
0.00000
.00472b_/
-11
 a/  x 10-3.
 b/  Per stack?  to obtain total for kiln, multiply by 7.
 c_/  Per stack;  to obtain total for kiln, multiply by 8.
                                      115

-------
                                   TABLE D-9

                     SUMMARY OF RESULTS (BENZ|V]PHENANTHRENE)
NAME

DESCRIPTION
DATE OF RUN
VMSTD VOL DRY GAS-STD COND
PMOS PERCENT MOISTURE BY VOL
TS AVG STACK TEMPERATURE
OS STK FLOWRATE* DRY,STD CN
QA ACTUAL STACK FLOWRATE
PERI PERCENT ISOKINETIC
PART
MF
CAN
CAT
CAW
PART
MT
CAO
CAU
CAX
1C
ICULATES — PARTIAL CATCH
PARTICULATE NT-PARTIAL^/
PART. LOAD-PTL«STD CN2/
PART. LOAD-PTL.STK CN3./
PART 1C UMIS-PARTIAL-
ICULATES -- TOTAL CATCH
PARTICULATE NT-TOTAL^ /
PART. LOAD-TTLtSTD CN~/
PART. LOAD-TTL»STK CN~
PARTIC EMIS-TOTAL-'
PERC IMPINGER CATCH
UNITS

DSCF
OEG.F
DSCFM
ACFM

MG
GR/DSCF
6R/ACF
LB/HR

MG
GR/DSCF
GP/ACF
LB/HR
?
12-03-75 1
15.64
25.0
150.0
42
67
93.5

15.40
.01516
.00968
.00552b-/

15.40
.01516
.00968
.00552^/
0.00
                                                           15.98
                                                            28.5
                                                           155.6
                                                               42
                                                               69
                                                            97.1
                                                            3.40
                                                          .00320
                                                          .00198
                                                          .00117.?-'
                                                           23.40
                                                          .02255
                                                          .01360
                                                          .00807-'
                                                           85.47
 13.64
  35.0
 163.8
    32
    60
 106.fl
 11.00
.01242
.00671
.00345^
 11.00
.01242
.00671
  0.00
a/  x 10-3.
b/  Per stack; to obtain total for kiln, multiply by 8.

-------
                             TABLE D-9  (Concluded)
NAME       DESCRIPTION

        DATE  OF  RUN
UNITS       B          10           12

         12-06-75  12-07-75  12-08-75
VMSTD VOL DRY GAS-STO CONO
PMOS
TS
QS
QA
PERI
PART
MF
CAN
CAT
CAW
PART
MT
CAO
CAU
CAX
1C
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATEt DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
ICULATES — MARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAU-PTL»STD CN
PART. LOAD-PTL.STK CN
PARTIC EMIS-PARTIAL
ICULATES — TOTAL CATCH
PARTICULATE WT-TOTAL-',
PART. LOAD-TTL»STD CN^/
PART. LOAD-TTL.STK CN^'
PARTIC EMIS-TOTAL2/
PERC IMPINOER CATCH
OSCF

OEG.F
OSCFM
ACFM


MO
GR/OSCF
GR/ACF
LB/HR

MG
GR/DSCF
GR/ACF
LB/HR

OSCF

OEG.F
OSCFM
ACFM

11.43
?8.5
155.0
35
57
95.0
12.49
38.9
204.4
28
59
111.0
8.24
32.3
258.6
24
49
100.5
MG
GR/OSCF
GR/ACF
LB/HR
0.00
0.00000
0.00000
0.00000
0.00
0.00000
0.00000
0.00000
0.00
0.00000
0.00000
0.00000
                                                 19.80
                                                .02667
                                                .01629
                                                .00798k/
                                                100.00
                        10.30
                      .01270
                      .00613
                      .00309£/
                      100.00
a/  x 10-3.
]>/  Per stack;  to obtain total for kiln, multiply by 7.
cj  Per stack;  to obtain total for kiln, multiply by 8.
 27.30
.05101
.02498
.01040k/
100.00

-------
                                                       TABLE  D-10
                                 SUMMARY OF RESULTS—METRIC  UNITS  (BENZ[£]PHENANTHRENE)
oo
NAME

VMSTM
PMOS
TSM
QSM
QAM
PERI
EA
PARTI
MF
CANM
CATM
CAWM
DESCRIPTION
DATE OF RUN
VOL DRY GAS-STD COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE, DRYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT 1SOKINETIC
PERCENT EXCESS AIR
CULATF.S -— PARTIAL CATCH
PARTICIPATE WT-PARTIAL^
PART. LOAD-PTL.STD CN^/
PART. LOAO-PTL,STK CN^7
PARTIC t MIS-PARTIAL-7
UNITS

NCM

DEG.C
NM3/MIN
M3/MIN



MG
MG/NM3
M6/M3
KG/HR
?
12-03-75
.443
25.0
65.5
1.2
1.9
93.5
67

15.40
34.70
22.16
- .00250£7
4
12-04-75
.453
28.5
68,7
1.2
2.0
97.1
4?

3.40
7.50
4.52.
.00053-7
6
12-05-75
«3B6
35.0
73.2
.9
1.7
106.8
64

11.00
28.43
15.35
.00157k/
PARTICULATES — TOTAL CATCH
MT
CAOM
CAUM
CAXM
1C
PARTICULATE WT-TOTAL-7,
PART. LOAD-TTL«STD CN-7
PART. LOAD-TTLtSTK. CN^7
PARTIC EMIS-TOTAL-7
PERC IMPINGER CATCH
MG
MG/NM3
MG/M3
KG/HR

15.40
34.70
22.16
.002 5 Ok/
0.00
23.40
51.60
31.12
.00366k/
85.47
11.00
28.43
15.35
.00157k/
0.00
                al  x 10-3.
                b/  Per stack; to obtain total for kiln, multiply by 8.

-------
                           TABLE D-10  (Concluded)
NAME
VMSTM
PMOS
TSM
QSM
QAM
PERI
EA
          DESCRIPTION
       DATE OF  RUN
                           UNITS
                                    NCM
VOL DRY GAS-STO  CONO
PERCENT MOISTURE BY  VOL
AVO STACK TEMPERATURE     OEG.C
STK FLOWRATE* ORYtSTD CN NM3/MIN
ACTUAL STACK FLOWRATE    M3/MIN
PERCENT ISOKINETIC
PERCENT EXCESS AIR
PARTICULATES —  PARTIAL CATCH

MF     PARTICULATE  WT-PARTIAL
CANM   PART. LOAD-PTL»STD CN
CATM   PART. LOAD-PTL.STK CN
CAWM   PARTIC EMIS-PARTIAL

PARTICULATES —  TOTAL  CATCH
MT
CAOM
CAUM
CAXM
1C
       PARTICULATE  WT
       PART. LOAD-TTL.STD
       PART. LOAD-TTL.STK
       PARTIC  KMIS-TOTAL2/
       PERC  IMPINGER CATCH
                                     MG
                                 MG/NM3
                                  MG/M3
                                  KG/HR
                              MG
                          MG/NM3
                           MG/M3
                           KG/HR
B
12-06-75
.324
2fl.5
6B.3
1.0
1.6
95.0
39
0.00
0.00
0.00
0.00000
19.80
61.03
37.27
.00362V
100.00
10
12-07-75
.354
38.9
95.8
.8
1.7
111.8
14
0.00
0.00
0.00
0.00000
10.30
29.07
14.03
.ooi4o£'
100.00
12
12-08-75
.233
32.3
125.9
.7
1.4
100.5
-11
0.00
0.00
0.00
0.00000
27.30
116.72
57,16
.00472V
100.00
at/  x 10-3.
b/  Per stack; to obtain total for kiln, multiply by 7.
£/  Per stack; to obtain total for kiln, multiply by 8.

-------
                                          TABLE D-ll





                           BENZ(V]PYRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG
50
.F)
.0
PORT-
PO

1
2
4
3
5
6
7
8
INT

1
1
1
1
1
1
1
1
ATMOS
PRES
(I.H6)
29.31
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(OCF) (
854.97
857.01
859.01
860.85
863.15
865.45
867.35
869.71
RUN- 4
H20 PARTIC
COND WT-PTL
(ML)
134.4
DELTA
P
I.H20)
.004
.008
.008
.007
.011
.ail
.006
.011
(M6)
3.40£/
DELTA
H
DATE- 12-04-75
PARTIC STACK INIT
WT-TTL AREA VOL

-------
                                       TABLE D-12





                     BENZ[V]PYRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG.F)
50.0
PORT-
POINT

1 1
2 1
4 1
3 1
5 1
6 1
7 1
8 1
ATMOS
PRES
(I.HG)
29.25
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
-o.oo
METER
VOL
(DCF) (]
871.25
872.97
874.84
876.42
878.15
879.83
882.05
883,70
RUN- 6 DATE- 1
H?0 PARTIC PARTIC
COND
( Ml )
154.8
DELTA
P
I.H?0)
.004
.006
.006
.004
.006
.006
.010
.006
WT-PTL WT-TTL
(MG)
3.2C
DELTA
H
(I.H20)
.300
.350
.450
.300
.400
.400
.700
.400
(MG
'-' ->•
TEMP
IN
(D.F) (
6fl.O
67.0
67.0
69.0
66.0
68.0
70.0
70.0
>
2o£/
TEMP
OUT
D.F)
70.0
67.0
67.0
69.0
67.0
68.0
70.0
70.0
2-05-75
STACK INIT
AREA
(FT2)
.20
TRAIN
VAC
(I.HG)
5.0
5.0
5.0
5.0
7.0
8.0
10.5
7.0
VOL
(DCF)
869.81
STACK
TEMP
(D.F)
155.0
155.0
150.0
160.0
160.0
165.0
180*0
185.0
PERC PERC PFRC PITOT
02 C02
DRY DRY
9.2 17.2
S.GEL PROBE
TEMP T OIA
(D.F) (IN)
70.0 .600
.600
.600
.600
.600
,600
.600
.600
CO TUHE
DRY COEF
4.1 .850

VEL
(FPM)
250.0
300.0
300.0
250.0
300.0
300.0
400.0
300.0
x 10-3.

-------
Ni
                                                       TABLE D-13

                                        BENZ[ji]PYRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG.F)
40.0
PORT-
POINT

4 1
3 1
5 1
6 1
7 I
8 1
1 1
ATMOS
PRES
(I.HG)
29.65
SAMP
TIME
( M I N )
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
885.07
886.77
888.41
889.80
891.43
89J.04
894.69
RUN- 8
H20 PARTIC
COND
(ML)
96.1
DELTA
P
I.HPO)
.004
.006
.006
.004
.006
.006
.006
WT-PTL
(MO)
0.00£/
HELTA
H
U.H20) (
.250
.400
.400
.250
.400
.400
.400
DATE- 12-06-7b
PARTIC STACK
WT-TTL


(

TEMP
IN
D.F
44.
42.
43.
44.
44.
49.
50.

)
0
0
0
0
0
0
0
MG)
e.eok/
TEMP
OUT
(D.F)
46.0
42.0
43.0
44.0
44.0
49.0
50.0
AREA
(FT?)
,?0
TRAIN
VAC
(I.HG)
4.0
4.0
4.0
6.0
5.0
9.0
9.0
INIT
VOL
( DCF )
883.70
STACK
TEMP
(D.F)
150.0
140.0
155.0
145.0
160.0
175.0
160.0
PERC PERC PERC PITOT
02 C02
DRY DRY
6.4 16.1
S.GF.L PROBE
TEMP T DIA
(D.F) (IN)
.600
.600
.600
70.0 .600
.600
.600
.600
CO TUBE
DRY COEF
1.5 .850

VEL
(FPM)
250.0
300.0
300.0
P50.0
300.0
300.0
300.0
             a/   Not  detectable.
             b/   x  10-3.

-------
10
CO
                                                       TABLE  D-14


                                        BENZlVJPYRENE DATA AND CALCULATED VALUES
ATMOS
TEMP
(DG.
40,
F)
0
PORT-
POI

1
4
3
5
6
7
8
2
NT

1
1
1
1
1
1
1
1
ATMOS
PRES
(I.HG)
29.65
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
896.12
898.14
899.48
901.06
902.40
903.95
905.49
906.78
RUN- 10
H?0 PARTIC
COND
(ML)-
168.0
DELTA
P
I.H20)
.004
.010
.004
.006
.004
.006
.005
.005
WT-PTL
(MG)
o.ooiL/
DELTA
H
(I.H20) (
.250
.650
.250
.300
.250
.300
.300
.200
DATE- 12-07-75
PARTIC STACK INIT
WT-TTL
(MG
16. i
TEMP
IN
D.F) (
42.0
41.0
41.0
42.0
44.0
46.0
48.0
49.0
)
30_/
TEMP
OUT
D.F)
45.0
41.0
41.0
42.0
44.0
46.0
48.0
49.0
AREA
(FT2)
.20
TRAIN
VAC
(I.HG
5.0
11.0
7.0
7.0
7.0
8.0
6.0
8.0
VOL
(DCF)
894.80
STACK
TEMP
) (D.F)
180.0
205.0
165.0
175.0
175.0
185.0
215.0
335.0
PERC PERC PERC PI TOT
02
DRY
5.1 1
S.GEL
TEMP
(D.F)


50.0
60.0


70.0

C02
DRY
8.2
PROBE
T DIA
(IN)
.600
.600
.600
.600
.600
.600
.600
.600
CO TUBF
DRY COEF
5.5 .850

VEL
(FPM)
250.0
400.0
250.0
300.0
250.0
300.0
300.0
300.0
             a/   Not  detectable.
             b/   x 10-3.

-------
to
-p-
                                                        TABLE D-15




                                        BENZ[V]PYRENE  DATA AND CALCULATED VALUES
ATMOS
TEMP

40.0
PORT-
POINT

1 1
?. 1
4 1
3 1
5 1
6 1
7 1
ATMOS
PRES
(I.HG)
29.35
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
0.00
METER
VOL
(DCF) (
909.38
910.51
911.59
912.73
913.88
915.17
916.16
RUN- 12
H20 PARTIC
COND WT-PTL
(ML>
83.0
DELTA
P
I.H20)
.005
.003
.003
.003
.004
.004
.003
(M6)
o.ool/
DELTA
H
DATE- 12-08-75
PARTIC STACK INIT
WT-TTL AREA VOL

-------
                                     TABLE D-16
                             BENZ[a]PYRENE EMISSION DATA
NAME

DN
TT
PB
PM
VM
TM
VMSTD
VH
VWV
PMOS-
MD
PC02
P02 ... -
PCO
PN2
MWD
MW
CP
DPS .
TS
NP
PST _ ...
PS
vs
A C
Aw 	 —
OS
QA
PERI- -
MF
MT
1C
CAN
CAO
CAT
CAU
CAW
CAX
EA
DESCRIPTION
DATE OF RUN
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD CONO
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL* DRY
PERCENT 02 OY VOL » DRY
PERCENT CO BY VOL » DRY
PERCENT N2 BY VOL» DRY
MOLECULAR WT-DR-Y -STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING POINTS
STATIC PRES- OF STACK 	
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
CTAPK ARFA
. o 1 A V-FV-- -Mrvt^M 	 - - - — — •- - - — - - -
STK FLOWRATE, DRY»STD CN
ACTUAL STACK FLOWRATE
PERCENT iSOKlNtTIC 	 -
PARTICULATE WT-PARTI AIJL/
PARTICULATE WT-TOTAL^'
PERC IMPINGER CATCH -.
PART. LOAD-PTL»STD CN^',
PART. LOAD-TTL»STD Cl£'
PART. LOAD-PTLtSTK . CN2/,
PART. LOAD-TTL,STK CN-7
PARTIC EMIS-PARTIAlJ^
PARTIC EM1S-TOTAL-'
PERCENT EXCESS AIR
UNITS

IN
MIN
IN.HG
IN.H20
DCF
OEG.F
DSCF
ML
SCF









IN.H20
DEG.F

IN.HG
IN.HG
FPM
TN9
- I PI C
DSCFM
ACFM

MG
MG

GR/DSCF
GR/DSCF
GR/ACF
GR/ACF
LB/HR
LB/HR

4
12-04-75
.600
40.0
29.31
.606
16.20
67.1
15.98
134.4
6.37
28.5
.715
15.0
7.3
2.9
74.8
30.69
27.07
.850
.008
155.6
8
-0.00
29.31
346
PQ
£ *
42
69
97.1
3.40
14.30
76.22
.00328
.01378
.00198
.00831
.00117^
.00493b-/ •
42
6
12-05-75
.600
40.0
29.25
.412
13.89
68.3
13.64
154.8
7.34
35.0
.650
17.2
9.2
4.1
69,5
31.12
26.53
,850
.006
163.8
8
-0.00
29.25
300
PO
c ^
32
60
106.8
3.20
7.20
55.56
.00361
.00813
.00195
.00439
.0010()b>/
.00226-7
64
8
12-06-75
,600
35.0
29.65
.357
10,99
45.3
11.43
96.1
4,56
28.5
.715
16.1
6.4
U5
76.0
.-- 30.83
27.18
.850
.006
155.0
7
-0.00
29.65
286
29
.... f*. r
35
57
95.0
0.00
6.60
100.00
0.00000
.00889
0.00000
.00543
0.00000
.002 6^
39
a/  x 10-3.
b/  Per stack; to obtain total for kiln, multiply by 8.
£/  Per stack; to obtain total for kiln, multiply by 7.
                                         125

-------
 NAME
              TABLE D-16  (Concluded)

   DESCRIPTION             UNITS
                                        10
_DN   —
 TT
 PB
.PM .........
 VM
 TM
 VMSTD-
 VW
 VWV
PMOS ..
 MD
 PC02
 P02. ...
 PCO
 PN2
_MWD
 MM
 CP
 OPS  _
 TS
 NP
 DATE  OF  RUN

. .PROS£_4LIP—D-I-AME-T-E-8	
 NET TIME OF RUN
 BAROMETRIC PRESSURE
_AVG ORIFICE -P-RES-&ROP	
 VOL DRY  GAS-METER COND
 AVG GAS  METER TEMP
-V-01	DR-Y—GAS^SJ.O - COND	
 TOTAL H20 COLLECTED
 VOL H20  VAPOR-STD COND
 .PERCENT... M.01SIUHE_flY. -VOL —
 MOLE  FRACTION DRY GAS
 PERCENT  C02 BY VOL, DRY
_P£RC£NI...D2_By-_V£lL4--DA.Y	
 PERCENT  CO BY VOL» DRY
 PERCENT  N2 BY VOLt DRY
                                            12-07-75
                        12

                    12-08-75
                             MIN
                           IN.HG
   DCF
 DEG.F
- DSCF-
    ML
   SCF
 PS
 vs
-AS
 OS
 QA
.P£R1_.
 MF
 MT
 MOLECULAR WT-STK GAS
 PITOT  TUBE COEFFICIENT
-^AVG--SJK-J/ELOCIT-Y HEAD	WUW20 .
 AVG  STACK TEMPERATURE      DEG.F
 NET  SAMPLING POINTS

 STACK  PRESSURE* ABSOLUTE   IN.HG
 AVG  STACK GAS VELOCITY       FPM
._S TACK—AREA	I-N2-
 STK  FLOWRATE» DRY,STD CN   DSCFM
 ACTUAL  STACK FLOXRATE
._£EftCENl_I5 OJU-biEJ. J C	a i
 PARTICULATE WT-PARTIAIT
 PARTICULATE WT-TOTAL-
                            ACFM
                               MG
                               MG
                                         40.0
                                        29.65
                                        -,312-
                                        11.98
                                         44.3
                                        -1-2,4-9
                                        168.0
                                         7.96
                                       .  38^9.
                                         .611
                                         18.2
                                          5*1
                                          5.5
                                         71.2
                                        31.12
                                        26.01
                                         .850
                                         .4)05-
                                        204.4
                                            8
                                        .--0...00
                                        29.65
                                          294
                                           29..
                                           28
                                           59
                                         0.00
                                        16.80
                        35.0
                       29.35
                                                  7.99
                                                  44.2
                                                  6*2-4
                                                  83.0
                                                  3.93
                                                  -32.. 3.
                                                  .677
                                                  22.3
                                                   -U4-
                                                   6.7
                                                  69.9
                                                 3U6-1-
                                                 27.21
                                                  .850
                                                  ..003
                                                 258.6
                                                     7
                       29,35
                         243
                   ----------- 29
                          24
                          49
                   ---- 10.0.5-.
                        0.00
                       32.20
 CAN
 CAO
 .CAT...... -
 CAU
 CAW
 CAJ< ___
 EA
 PART.  LOAD-PTL.STD CN~/  GR/DSCF
 PART.  LOAD-TTL»STD CN£/  GR/DSCF
 PART.  LOAD-TTL,STK CN£    GR/ACF
 PARTIC EMIS-PARTIA^-7       LB/HR
_..PART.IC__£MlSr-j
                                     0.00000
                                      .02072
                                    ^0 -.00000
                                      .01000
                                     0.00000
PERCENT EXCESS  AIR
                                            14
                     0.00000
                      .06016
                    -0.00000
                      .02946
                     0.00000
                    	01227£/
                         -11
£/  X 10-->.
b_/  Per stack;  to obtain total for kiln, multiply by 8.
£/  Per stack;  to obtain total for kiln, multiply by 7.
                               126

-------
                               TABLE D-17

                 BENZJVJPYRENE EMISSION DATA (METRIC RESULTS)
NAME    .. -DESCRIPTION  	

        DATE OF RUM
-.-.	UNITS	—	4-	-6			-8	

             12-04-75  12-05-75  12-06-75
DN
TT
PB.~-
PM
VM
T-M	
VMSTM
VW
VWrt..
PMOS
MD
P.C02 —
P02
PCO
PN2	
MUD
MW
CP-	
DPS
TSM
NP	
PST
PS
VSM	
AS
QSM
QAR--
PERI
MF
MX	
1C
CANM
CAOM_
CATM
CAUM
CAWM_
CAXM
EA
 PROBE TIP  DIAMETER
 NET TIME OF  RUN
. BARSMEIRJLC-P-RESSURE	
 AVG ORIFICE  PRES DROP
 VOL DRY GAS-METER COND
_A V-G -GAS-METER—T-E-MP-	
        VOL DRY GAS-STD  COND
        TOTAL H20 COLLECTED
        V-QL -H20-.V.APOR«SIO-COND- --
        PERCENT MOISTURE BY VOL
        MOLE  FRACTION  DRY GAS
        PER.CFJJJ- C02 -BY-tf-Ol^-DR-Y- -
        PERCENT 02  BY  VOL» DRY
        PERCENT CO  BY  VOL» DRY
                                       IN
                                     WIN
                                   I1»UHG
                                  IN.H20
                                     DCF
      NCM
       ML
      NM3
                 .600
                 40.0
                29,31
                 .606
                16.20
 MOLECULAR  WT-DRY STK  GAS
 MOLECULAR  rtT-STK GAS
.-PJLTOJ-JUaF CnFFF-J.C.I£AiT- __
 AVG  STK  VELOCITY HEAD
 AVG  STACK  TEMPERATURE
..NEI-SAMPL ING-.P-OIN-TS	
 STATIC PRES OF STACK
 STACK PRESSURE* ABSOLUTE
. .AV-G. -SIACK-6AS VEL OCI-T-Y- -
 STACK AREA
 STK  FLOWRATEi DRY,STD CN
--ACT-U AL—SIACK-F-UD WRA T-E—
 PERCENT  ISOKINETIC
 PARTICULATE 	
_ PART4£ULAi£.-W.T--r..n).XAL-/ -—
 PERC  IMPINGER CATCH    /
 PART. LOAD-PTL»STD CN-/
__P-Afi-T-.. -LaAD.-T Ji^-S-IO-CN-/
 PART. LOAD-PTL»STK CN~/
 PART. LOAD-TTL»STK CN~
                    ,a/
                                   IN.H20
                                   DEG.C
                                    IN.HG
                                    IN.HG
                                  -4H/M-IN -
                                      IN2
                                  NM3/MIN
                                ,
                     WT-PARTIAL-
       MG
._ P-AR TIC.. .EMIS'-P-ARTTA^L-
 PARTIC EMIS-TOTAL-7
 PERCENT  EXCESS AIR
 MG/NM3
_MG/NM3-
  M6/M3
  MG/M3
	tG/HR-
  KG/HR
                                               .002242.7
                                                   42
                            4.47
                           10.05
                          .00046k/
                          ,00102k/
                              64
  100.00
    0.00
-.-20,34-
    0.00
   12.42
.^4)000-0
  .0012!£/
      39
 a/  x 10-3.
 b_/  Per stack; to obtain total for kiln, multiply by 8.
 £/  Per stack; to obtain total for kiln, multiply by 7.
                                   127

-------
                       TABLE D-17  (Concluded)
NAME    -   DESCRIPTION-

        DATE  OF RUN
UNITS        10
         12-07-75   12-08-75
DN
TT
PB .
PM
VM
TM
VMSTM
VW
VWM
PMOS
MD
PC02
P02
PCO
PN2 	
MWD
MW
CP ...
DPS
TSM
NP ...
PST
PS
VSM
AS
OSM
QAM
PERI
MF
MT
1C
CANM
CAOM
CATM
CAUM
CAWM
CAXM
EA
PROBE TIP DIAMETER
NET TIME OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP- -
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND -
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT.. C02 8Y- VOL, DRY
PERCENT 02 BY VOL, DRY
PERCENT CO BY VOL, DRY
PERCENT- N2 BY VOL, DRY
MOLECULAR WT-ORY STK GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
.NET SAMPLING POINTS
STATIC PRES OF STACK
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY-
STACK AREA
STK FLOWRATE, DRY,STD CN
ACTUAL -STACK FLOWRATE.
PERCENT ISOKINETIC /
a /
PARTICULATE WT-PARTIAL"
PARTICULATE WT-TOTAll-'
PERC IMPINGER CATCH /
PART. LOAD-PTL,STD CN~/
PART. LOAD-TTL»STD CN~/
PART. LOAD-PTL,STK CN^/
PART. LOAO-TTL»STK CN~
PARTIC EMIS-PARTIALr
PARTIC EMIS-TOTAtr^
PERCENT EXCESS AIR
IN
MIN
IN.HG
IN.H20
DCF
DEG.F
NCM
ML
NM3









IN.H20
DEG.C

IN.HG
IN.HG
M/MIN
IN2
NM3/MIN
M3/MIN

MG
MG

MG/NM3
MG/NM3
MG/M3
MG/M3
KG/HR
KG/HR

.600
. 40.0
29.65
.312
11.98
44.3
.35
168.0
.23-
38.9
.611
18.2
5.1
5.5
71.2
31.12
26,01
.850
,005
95.8
8
-0.00
29.65
89.6
29
.8
1.7
111.8
0.00
16.80
100.00
0.00
47.42
0.00
22.89
0.00000
.00228J2/
14
.600
35.0
29.35
.193
7.99
44.?
.23
83.0
.11
32.3
.677
22.3
1.1
6.7
69.9
31.61
27.21
.850
.003
125.9
7
-0.00
29.35
- 74,0
29
.7
1,4.
100.5
0.00
32.20
100.00
0.00
137.67
0.00
67.4?
0.00000
.005 5 6£/
-11
 a/   x 10-3.
 b/   Per stack?  to  obtain total  for kiln, multiply by 8.
 c/   Per stack;  to  obtain total  for kiln, multiply by 7.
                                 128

-------
                                                TABLE D-18


                                      SUMMARY OF RESULTS (BENZIVJPYRENE)
NJ
              NAME       DESCRIPTION

                     DATE  OF RUN
UNITS
VMSTD VOL DRY GAS-STD COND
PMOS PERCENT MOISTURE BY VOL
TS AVG STACK TEMPERATURE
OS STK FLOwRATE.-DRYtSTD CN
QA ACTUAL STACK FLOWRATE
PERI PERCENT ISOKINETIC
PARTICULATES — PARTIAL CATCH
a/
MF PARTICULATE NT-PARTIAL",
CAN PART. LOAD-PTL.STD CN-'
CAT PART. LOAD-PTL»STK CN-7
CAW PARTIC EMIS-PARTIAL-7
PARTICULATES — TOTAL CATCH
MT PARTICULATE WT-TOTAL" a/
CAO PART. LOAD-TTL«STD CN~/
CAU PART. LOAD-TTL.STK7 CN-
CAX PARTIC EMIS-TOTAL-
IC PERC IMPINGER CATCH
DSCF
DEO.F
DSCFM
ACFM
MO
GR/DSCF
GR/ACF
LB/HR
MG
GR/DSCF
GR/ACF
LB/HR
         12-04-75   12-05-75   12-06-75
15.98
28.5
155.6
69
97.1
13.64
35.0
163.8
IP
(J C.
60
106.8
11.43
28.5
155.0
35
- ^j ^f
57
95.0
MO
GR/DSCF
GR/ACF
LB/HR
3.40
.00328
.00198
.00117-'
3.20
.00361
.00195
.ooiooH/
0.00
0.00000
0.00000
0.00000
                                                              14.30
                                                             .01378
                                                             .00831
                                                             .00493^
                                                              76.22
                        7.20
                      .00813
                      ,00439
                      . 002 26^
                       55.56
              a/  x 10-3.
              b/  Per stack; to obtain total for kiln, multiply by 8.
              £/  Per stack; to obtain total for kiln, multiply by 7.
  6.60
.00889
.00*43
.00266£/
100.00

-------
                       TABLE D-18  (Concluded)
NAME       DESCRIPTION
        DATE OF RUN
UNITS       10          12

         12-07-75   12-08-75
VMSTD
PMOS
TS
OS
OA
PERI
PARTI
MF 	
CAN
CAT
CAW
VOL DRY GAS-STD COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE, DRYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
CULATES — PARTIAL CATCH
PARTICULATE WT-PARTIAL
PART. LOAD-PTL«STD CN
PART. LOAD-PTL,STK CN
PARTIC EMIS-PARTIAL
DSCF

DEG.F
DSCFM
ACFM


MG
GR/DSCF
GR/ACF
LB/HR
PARTICULATES — TOTAL CATCH
.. -
MT
CAO
CAU
CAX
1C
- 	 a/
PARTICULATE WT-TOTAL" a/
PART. LOAD-TTL.STD CN~/
PART. LOAD-TTL»STK CN~
PARTIC EMIS-TOTAL^7
PERC IMPINGER CATCH

MG
GR/DSCF
GR/ACF
LB/HR

OSCF

OEG.F
DSCFM
ACFM

12.49
38.9
204.4
28
59
111.8
8.24
32.3
258.6
24
49
100.5
                                                 0.00
                                              0.00000
                                              0.00000
                                              0.00000
                                                16.80
                                               .02072
                                               .01000
                                               .00504k/
                                               100.00
a/  x 10-3.
b/  Per stack; to obtain total for kiln, multiply by 8.
£/  Per stack; to obtain total for kiln, multiply by 7.
                        0.00
                     0.00000
                     0.00000
                     0.00000
                       32.20
                      .06016
                      .02946
                      .01227£/
                      100.00

-------
                                      TABLE  D-19

                   SUMMARY OF RESULTS—METRIC  UNITS  (BENZ[£]PYRENE)
NAME

DESCRIPTION
DATE OF RUN
VMSTM VOL DRY GAS-STD COND
PMOS
TSM
QSM
QAM
PERI
EA
PART
MF
CANM
CATM
CAWM
PART
MT
CAOM
CAUM
CAXM
1C
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE, DRY,STO CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PERCENT EXCESS AIR
ICULATES — PARTIAL CATCH
PARTICULATE. WT-PARTI AL-/
PART. LOAD-PTLtSTD CN^/
PART. LOAD-PTL,STK CN-'
PARTIC EMIS-PARTIAL-
ICULATES — TOTAL CATCH
a/
PARTICULATE WT-TOTAL~ a/
PART. LOAO-TTL»STD CN^/
PART. LOAD-TTL,STK. CN~
PARTIC EMIS-TOTAL-'
PERC IMPINGER CATCH
UNITS

NCM

DEG.C
NM3/M1N
M3/MIN



MO
MO/NM3
MG/M3
KG/HR

MO
MO/NM3
MG/M3
KG/HR

4
12-04-75
.453
?8.5
68.7
1.2
2.0
97.1
42

3.40
7.50
4,52
.00053^/

14.30
31.53
19.01
.00224k/
76.22
6
12-05-75
,3ft6
35.0
73.2
.9
1.7
106.6
64

3.20
8.27
4.47
.00046k/

7.20
18.61
10.05
.00102k/
55.56
8
12-06-75
.324
28.5
68.3
1.0
1.6
95.0
39

0.00
0.00
0.00
0.00000

6.60
20.34
12.42
,00121-/
100.00
a   x 10-3.
b/  Per stack;  to obtain total for kiln,  multiply by 8.
c/  Per stack;  to obtain total for kiln,  multiply by 7.

-------
                    TABLE D-19  (Concluded)
NAME
VMSTM
PMOS
TSM
QSM
QAM
PERI
EA
DESCRIPTION
        DATE OF RUN
                           UNITS
                          NCM
10
12
VOL DRY GAS-STD  COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE     DEG.C
STK FLOWRATE*  DRY.STD CN NM3/MIN
ACTUAL STACK FLOWRATE    M3/MIN
PERCENT ISOKINETIC
PERCENT EXCESS AIR
PARTICULATES — PARTIAL CATCH
MF      PARTICULAR WT-PARTIAL
CANM    PART.  LOAD-PTL,STD CN
CATM    PART.  LOAD-PTL.STK CN
CAWM    PARTIC EMIS-PARTIAL

PARTICULATES  — TOTAL CATCH
                                12-07-75   12-08-75
.354
38.9
95.8
.8
1.7
111.0
14
.233
32.3
125.9
.7
1.4
100.5
-11
MG
M6/NM3
MG/M3
KG/HR
0.00
0.00
0.00
0.00000
0.00
0.00
0.00
0.00000
af  x 10-3.
jb/  Per stackj to obtain total for kiln, multiply by 8.
c/  Per stack; to obtain total for kiln, multiply by 7.
MT
CAOM
CAUM
CAXM
1C
PARTICULATE WT-TOTAL" a/
PART. LOAD-TTL»STD CN^/
PART. LC)AD-TTL,STK, CN~
PARTIC EM1S-TOTAL-
PERC-IMPINGER CATCH
MG
MO/NM3
MG/M3
KG/HR

16.80
47.42
22.89
.002 2 ak/
100.00
32.20
137.67
67.42
.00556£/
100.00

-------
                                              TABLE D-20
                               POM-LIKE MATERIAL DATA AND CALCULATED VALUES
                                  RUN-
                                  DATE- 12-03-75
         ATMOS
         TEMP
        (DG.F)

         40.0
 ATMOS
 PRES
(I.HG)
 STACK   H20
  VAC   COND
(I.H20)  (ML)
PARTIC   PARTIC   STACK  INIT   PERC PERC PERC  PITOT
WT-PTL   WT-TTL    AREA   VOL    02   C02   CO    TUBE
 (M6)      (MO)      (DCF)    DRY  DRY   DRY   COEF
 29.31   0.00  109.8   345.00£/   376.00£/    .20  837.66  9.2  11.0  1.9  .850
UJ
PORT-
POINT

1
2
4
3
5
6
7
8

1
1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(OCF) (I
838.98
840.69
842.82-
845.03
847.27
849.49
851.22
853.23
DELTA
P
.H?0)
.005
.006
.009
.009
.011
.011
.004
.008
DELTA
H
(I.H20)
.270
.400
.650
.700
.700
.650
.450
.550
TEMP
IN
(D.F)
43.0
49.0
53.0
58.0
62.0
64.0
65.0
65.0
TEMP
OUT
(D.F)
43.0
49.0
53.0
60.0
62.0
64.0
66.0
65.0
TRAIN
VAC
(I. MO)
8.5
5.0
5.0
6.0
9.0
7.0
12.0
12.0
STACK
TEMP
(D.F)
140.0
145.0
130.0
140.0
160.0
155.0
165.0
165.0
                                                         TEMP  T DIA
                                                        
-------
                                      TABLE D-21
                        POM-LIKE MATERIAL DATA AND CALCULATED VALUES
                           RUN-
                                 DATE- 12-04-75
 ATMOS  ATMOS  STACK    H20

 TEMP   PRES    VAC    COND

(OG.F) (I.HO) (I.H20-)  (ML)
 50.0
29.31
0.00  134.4
PORT-
POINT

1
2
4
3
5
6
7
8

1
1
1
1
1
1
1
1
SAMP
TIME
(M
5
5
5
5
5
5
5
5
IN)
.00
.00
.00
.00
.00
.00
.00
.00
METER DELTA
VOL P
(DCF) (I.H20)
854,
857,
859,
860,
863,
865,
867,
869,
,97
,01
,01-
,85
as
,45
,35
,71
.004
.008
.008
.007
.011
.011
.006
.011
PARTIC   PARTIC   STACK  INIT
WT-PTL   WT-TTL    AREA   VOL
 (MO)      (MO)    (FT2)  (DCF)
                                                        PERC PERC PERC  PITOT
                                                         02   C02  CO    TUBE
                                                         DRY  DRY  DRY   COEF
143. 00£
     £/   213. 00£/    .20  853.51   7.3 15.0  2.9   .850
ELTA
H
H20)
.500
.600
.550
.500
.700
.700
.600
.700
TEMP
IN
(D.F)
64
58
61
64
68
72
73
75
.0
.0
.0
.0
.0
.0
.0
.0
TEMP TRAIN
OUT VAC
(D.F
66.
60.
61.
64.
68.
72.
73.
75.
) (I. HO)
0
0
0
0
0
0
0
0
5.
7.
5.
5.
12.
9.
5.
13.
0
5
5
0
0
0
0
0
STACK S.GEL PROBE
TEMP TEMP T DIA
(D.F
150.
145.
160.
160.
165.
150.
160.
155.
) (D.F) (IN)
0
0
0
0
0
0
0
0
• 600
.600
.600
.600
.600
• 600
.600
.600
VEL
(FPM)
250
350
350
320
400
400
300
400
.0
.0
.0
.0
.0
.0
.0
.0
   a/
10-3.

-------
                                                       TABLE D-22
                                      POM-LIKE MATERIAL DATA AND CALCULATED VALUES
OJ
Ul
ATMOS
TEMP
(DG.F)
50.0
PORT-
POINT

1 1
2 1
4 1
3 1
5 1
6 1
7 1
8 1
ATMOS
PRES
(I.HG)
29.25
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
STACK
VAC
(I.H20)
-0.00
METER
VOL
(DCF) (
871.25
872.97
874.84
876.42
878.15
879.83
882.05
883.70
RUN- 6
H?0 PARTIC
COND WT-PTL

-------
                                      TABLE D-23
                        POM-LIKE MATERIAL DATA AND CALCULATED VALUES
                           RUN-   8
                           DATE-  12-06-75
 ATMOS  ATMOS
 TEMP   PRES
(DG.F) (I.H6)
 STACK   H20
  VAC   COMD
(I.H20) (ML)
PART 1C
WT-PTL
 (MG)
PARTIC
WT-TTL
 (MG)
 40.0   29.65   0.00    96.1
                   0.002/  191.OQb
STACK   INIT    PERC PERC PERC  PHOT
 AREA   VOL     02   C02  CO    TUBE
(FT2)   (DCF)    DRY  DRY  DRY   COEF

  .20   883.70   6.4 16.1  1.5   .850
PORT-
POINT

4
3
5
6
7
8
1

1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (1
885.07
886.77
888.41
889.80
891.43
893.04
894.69
DELTA
P
I.H20) (
.004
.006
.006
.004
.006
.006
.006
DELTA
H
I.H20)
.250
.400
.400
.250
.400
.400
.400
TEMP
IN
(D.F)
44.0
42.0
43.0
44.0
44.0
49.0
50.0
TEMP TRAIN
OUT VAC
(D.F) I
46.0
42.0
43,0
44.0
44.0
49.0
50.0
tl.HG)
4.0
4.0
4.0
6.0
5.0
9.0
9.0
STACK S.GEL
TEMP TEMP
(D.F) (D.F)
150.0
140.0
155.0
145.0 70.0
160.0
175.0
160.0
PROBE
T DIA
(IN)
.600
.600
.600
.600
.600
.600
.600
VEL n
(FPM) g£p!l
250.0 "J
300.0 ^«^
300.0
250.0
300.0
300.0
300.0
aj  Not detectable.
b/  x 10-3.

-------
                                              TABLE D-24
                                POM-LIKE MATERIAL DATA AND CALCULATED VALUES
                                   RUN-    10
                                         DATE-  12-07-75
CO
 ATMOS  ATMOS  STACK    H20    PARTIC   PARTIC   STACK  INIT
 TEMP   PRES    VAC    CONO    WT-PTL   WT-TTL    AREA   VOL
(06, F) (I.HG)  (I.H20)  (ML)     (MG)      (MG)    (FT2)  (DCF)
                                                                        PERC PERC PERC  PITOT
                                                                         02   C02  CO    TUBE
                                                                         DRY  DRY  DRY   COEF
 40.0
                29.65    0.00  168.0   160. 002/   416. 00£/    .20  894.80   5.1 18.?  5.5   .850
PORT-
PO

1
4
3
5
6
7
8
2
INT

1
I
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
896.12
898.14
899.48.
901.06
902.40
903.95
905.49
906.78
DELTA
P
I.H20)
.004
.010
.004
.006
.004
.006
.005
.005
DELTA
H
(I.H20)
.250
.650
- .250
.300
.250
.300
.300
.200
TEMP
IN
(D.F)
42.0
41.0
41.0
42.0
44.0
46.0
48.0
49.0
TEMP
OUT
(D.F)
45.0
41.0
41.0
42.0
44.0
46.0
48.0
49.0
TRAIN
VAC
(I.HG)
5.0
11.0
7.0
7.0
7.0
8.0
8.0
8.0
STACK
TEMP
(D.F)
180.0
205.0
165.0
175.0
175.0
185.0
215.0
335.0
S.GEL
TEMP
(D.F)


50.0
60.0

- -.
70.0
-
PROBE
T OIA
(IN)
.600
.600
.600
.600
.600
.600
.600
.600

VEL
(FPM)
250.0
400.0
250.0
300.0
250.0
300.0
300.0
300.0
         £'  x 10-

-------
                                               TABLE D-25
                                POM-LIKE MATERIAL DATA AND CALCULATED VALUES
                                   RUN-
                             12
                         DATE-  12-08-75
         ATMOS  ATMOS   STACK   H20    PARTIC
         TEMP   PRES     VAC   COND    WT-PTL
        (DG.F)  (I.HG)  (I.H20) (ML)      (MG)
         40.0
  29.35
0.00
                                  PARTIC   STACK
                                  WT-TTL    AREA
                                   (MG)    (FT2)
                                        INIT   PERC  PERC PERC PJTOT
                                         VOL    OH    C02  CO   TUBE
                                        (DCF)   DRY   DRY  DRY  COEF
83.0   448.OQ2/   795.00£/   .20   908.17  1.1 22.3   6.7  .850
CO
CO
PORT-
POINT

1
2
4
3
5
6
7

1
1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
909.38
910.51
911.59
912.73
913.88
915.17
916.16
HELTA
P
I.H20)
.005
.003
.003
.003
.004
.004
• 003
DELTA
H
(I.H20)
.250
.200
.200
.200
.150
.200
.150
TEMP
IN
(D.F)
51.0
46.0
42.0
44.0
40.0
41.0
45.0
TEMP
OUT
(D.F)
54.0
46.0
43.0
44.0
40.0
41.0
42.0
TRAIN
VAC
(I.HG)
5.0
10.0
4.0
6.0
10.0
4.0
10.0
STACK
TEMP
(D.F)
360.0
330.0
220.0
170.0
230.0
190.0
310.0
S.GEL PROBE
TEMP T DIA
(D.F) (IN)
.600
• 600
.600
.600
50.0 .600
.600
.600

VEL
(FPM)
300.0
250.0
220.0
220.0
240.0
250.0
220.0
          a/
             x
10-3.

-------
                                   TABLE D-26
                         POM-LIKE MATERIAL EMISSION DATA
NAME

DN
TT
PB
PM
VM
TM
VMSTD
VW
VWV
PMOS
MD
PC02
..P02....
PCO
PN2
MtalD. .
MW
CP
DP.S- ...
TS
HP
PST...
PS
vs
AS
-p*-«* 	 • — -
QS
QA
-PERI..
MF
MT
..1C— -
CAN
CAO
CAT
CAU
CAW
-CAX--
EA
DESCRIPTION
DATE OF RUN
PROBE T-IP--OI-AMETER 	 -
NET TIME OF RUN
BAROMETRIC PRESSURE
-AVG ORIF-ICE -PRE-S -DROP 	
VOL DRY GAS-METER COND
AVG GAS METER TEMP
-VOL -DRY .-GAS-STD -COND- 	 —
TOTAL H20 COLLECTED
VOL H20 VflPQR-STD COND
... PERCENT-. -MD.I ST-URE- BY VOL
MOLE FRACTION DRY GAS
PERCENT COS 8Y VOLt DRY
PERCENT -02- B-Y-VOL^ DRY. _
PERCENT CO BY VOL. DRY
PERCENT N2 BY VOL» DRY
MOLECULA«..-WJ.*Wt.Y-ST«--&AS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
...AVG-STK VELOCITY-HEAD 	
AVG STACK TEMPERATURE
NET SAMPLING POINTS
. -STAT I C . PR£S-OF~S-TACK- 	 -
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
STACK AkF_A
STK FLOWRATEt DRY,STD CN
ACTUAL STACK FLOWRATE
-..PERCENT ..JSOKJNEJIC 	 a/
PART1CULATE WT-PARTI.AIT
PARTICULATE WT-TOTAl^'
_.PEHC-JMPJN6£.R_CATCH- /
PART. LOAD-PTLiSTD CN-/
PART. LGAD-TTLtSTD CNj/
PART. .LOAD-PTL-*-STK 	 CN-^_.
PART. LOAD-TTL,STK CN^
PARTIC EMIS-PARTIAL-7
....PART 1C E-MIS-TCTA4.-7—
PERCENT EXCESS AIR
UNITS

I-N - -
MIN
IN.HG
IN.H20 -
DCF
DEG.F
- 	 DSCF —
ML
SCF



— - 	





-IN.H20
DEG.F

-IK. KG
IN.HG
FPM
IN? .....
	 — i 1^ ^
DSCFM
ACFM
MG
MG
GR/DSCF
GR/DSCF
GPVACF
GR/ACF
LB/HR
-4.-B/HR —
2
12-03-75
.600
40.0
29.31
.546
15.57
57.6
- 15.64
109.8
5.20
25.0
.750
11.0
9.2
1.9
77.9
30.13
27.10
.850
- - .00^
150.0
8
-0.00
29.31
333
	 29 •-
W 7
42
67
	 93.5.-
345.00
376.00
---8.24-
.33970
.37022
.21694
.23643
.i^'ee^7
	 .13477^-
67
4
12-04-75
- .-600-
40.0
29,31
-.606 	
16.20
67.1
- - 15.-9B -
134.4
6.37
- 2o.5
.715
15.0
	 7^3-
2.9
74.8
• -- 30.69 -
27.07
.850
	 - .003
155.6
8
---0.00
29.31
346
. -_?Q
l« J
42
69
	 97..1
143.00
213.00
- 32. *6
.13781
.20526
	 ,06309
,12377
.04932^
	 .07347-'-
42
6
12-05-75
.600
40.0
29.25
.4-12
13.89
68.3
	 1-3.64
154.8
7.34
- -35 . 0
.650
17.2
	 9.2
4.1
69.5
- 31.12
26.53
.850
.006
163.8
8
-0.00
29.25
300
... _ 	 ?Q
b. f
32
60
106.6
69.00
105.00
	 34-,-29
.07792
.11858
,04206
.06404
.02164k/
- .03294k/
64
a/  x 10-3.
b/  Per stack; to obtain total for kiln,  multiply by 8.
                                       139

-------
                            TABLE D-26  (Concluded)
NAME       DESCRIPTION
        DATE OF  RUN
UNITS
10
12
         12-06-75  12-07-75   12-08-75
DN 	
TT
PB
PM . ...
VM
TM
VMSTD-.
VW
VWV
PMQS .-
MD
PC02
P02 	
PCO
PN2
MWD
MW
CP
.DPS 	
TS
NP
PST___
PS
VS
A^
- MO •-• 	
QS
OA
PERI 	
MF
MT
J.C 	
CAM
CAO
CAT _
CAU
CAX._. -
EA
PROBE -TIP-.-O.IAMET-ER 	 •--
NET TIME OF RUN
BAROMETRIC PRESSURE
. AVG-.-ORIF.ICE -PRES .-DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
..VOL -OR*. GAS.-.STO-COND 	
TOTAL H?0 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT ..MOISTURE. ..BY.. .VOL
MOLE FRACTION DRY GAS
PERCENT C02 BY VOL» DRY
.._ P£R C£NT -Q2-B Y - V.Q-L-* - -DR Y
PERCENT CO BY VOL» DRY
PERCENT NE 3Y VOL» DRY
MOLECULAR-WT--DR-Y -STK. -GAS
MOLECULAR WT-STK GAS
PITOT TUBE COEFFICIENT
._AV.G -STK. VELOCITY .-HEAD 	 -
AVG STACK TEMPERATURE
NET SAMPLING POINTS
_STA.TJC-P.RES. .OF. ..STACK
STACK PRESSURE, ABSOLUTE
AVG STACK GAS VELOCITY
CT kCK AWT A
__J l.^4^^»\ — J^fl ^ M 	 	 	 	 	
STK FLOWRATEf DRY»STD CN
ACTUAL <;TACK FLOWRATE
... PERCENT- ...1S.QK-LNE.T.IC- — ,-
PARTICULATE WT-PARTIAL-
PARTICULATE WT-TOTAL-7
_P£RC— IMP-JJ^GEJ? -CAJCH 	 a/—
PART. LOAD-PTL»STD CN~/
PART. LOAD-TTL.STD CN~/
_ PAR T.. .LO AD.-.P JL-t STK_.CN- / .
PART. LOAD-TTL.STK CN~
PARTIC EMIS-PARTlAll-7
. P.ARUC. EKLS-TOTAl^' 	
PERCENT EXCESS AIR
- IN
MIN
IN.HG
IN.H20
DCF
DEG.F
- OSCF
ML
SCF
	


— ,. .




.-IN.H20
DEG.F

-. IN.HG
IN.HG
FPM
TM?
	 1 *VC •
DSCFM
ACFM
MG
MG
	 	 	
GR/DSCF
GR/DSCF
.GR/ACF..
GR/ACF
LB/HR
. LB/HR.

,6OO
35.0
29.65
,357
10.99
45.3
11.43 -
96.1
4.56
28,5-
.715
16.1
6,4
1.5
76.0
3#»<33
27.18
.850
. -...006-
155.0
7
. -0.00
29.65
286
50
	 C f '
35
57
95.0
0.00
' 191,00
~- 100.00-
0.00000
.25726
- 0.00000 .
.15711
0.00000
.07695^'...
39
•••600-
40.0
29.65
-.312 	
11.98
44.3
-12,49—
168.0
7.96
-38.9
.611
18.2
.__. S, 1 -—
5.5
71.2
. 31,12 	
26.01
.850
.005 -
204.4
6
.-0,00 •--.
29.65
294
po 	
2G
59
111.8 -
160.00
416.00
- ...61,54—-
.19734
.51308
.,0952-5 -
.24766
.04797£/
• .12472S/-
14
.6-00
35.0
29.35
	 .193
7.99
44.2
	 8. -24
83.0
3.93
32.3
.677
22.3
.. . . 1...1 .
6.7
69.9
	 31,61
27.21
.850
	 ,.0-03-
258. 6
7
... -o.oo
29.35
243
24
49
- • 100,5
448.00
795.00
	 43,65
.83702
1.48533
-.,40994
.72746
.17067k/
- -,30286k/
-11
 a/  x 10-3.
 b/  Per stack; to obtain total for kiln, multiply by 7.
 £/  Per stack; to obtain total for kiln, multiply by 8.
                                     140

-------
'NAME
ON
TT
PB
PM
VM
TM
VMSTM
VW
VWM
PMOS
MO
PC02
P02
PCO
PN2
MWD
MW
CP
OPS
TSM
NP
PST
PS
VSM
AS
QSM
0AM
PERI
MF
MT
 1C
CANM
 CAOM
 CATM
 CAUM
 CAWM
 CAXM
 EA
                               TABLE D-27
               POM-LIKE MATERIAL EMISSION DATA (METRIC RESULTS)
   DESCRIPTION

DATE OF HUN

PROBE TIP DIAMETER
NET TIMt OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRES DROP
VOL DRY GAS-METER COND
AVG GAS METER TEMP
VOL DRY GAS-STD COND
TOTAL H20 COLLECTED
VOL H20 VAPOR-STD COND
PERCENT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02 RY VOL» DRY
PERCENT 02 BY VOL, DRY
PERCENT CO BY VOL» DRY
PERCENT N2 BY VOL» DRY
MOLECULAR WT-DRY STK  GAS
MOLECULAR WT-STK GAS
P1TOT TURE COEFFICIENT
AVG STK VELOCITY HEAD
AVG STACK TEMPERATURE
NET SAMPLING- POINTS
STATIC PRES OF STACK
STACK PRESSURE* ABSOLUTE
AVG STACK- GAS VELOCITY
STACK AREA
STK FLOWRATEt DRY,STD  CN
ACTUAL STACK FLOWRATE
                          UNITS
                             IN
                            MIN
                          IN.HG
                         IN.H20
                            DCF
                          DEG.F
                            NCM
                             ML
                            NM3
PERCENT  ISOKINETIC
                      a/
PARTICULATE  WT-PARTIAlr
PARTICULATE  WT-TOTAll-'
PERC  IMPINGER CATCH  a/
       LOAO-PTL»STD CN~/
       LOAD-TTL»STD CN~/
       LOAD-PTL»STK
       LOAO-TTL»STK CN
PARTIC EMIS-PARTIAll/
PAPTIC tMlS-TOTAll-7
PERCENT EXCESS AIR
PART.
PART.
PART.
PART.
IN.H20
 DEG.C

 IN.HG
 IN.HG
 M/MIN
   IN2
NM3/MIN
M3/MIN

    MG
    MG

MG/NM3
MG/NM3
 MG/M3
 MG/M3
 KG/HR
 KG/HP.
?
12-03-75
.600
40.0
29.31
.546
15.57
57.6
.44
109.8
.15
25.0
.750
11.0
9.2
1.9
77.9
30.13
27.10
.850
.008
65.5
8
-0.00
29.31
101.4
29
1.2
1.9
93.5
345.00
376.00
8.24
777.34
847.19
496.43
541.04
.05609k/
.06113k/
67
4
12-04-75
.600
40.0
29.31
.606
16.20
67.1
.45
134.4
.18
28.5
.715
15.0
7.3
2.9
74.8
30.69
27.07
.850
.008
68.7
8
-0.00
29.31
105.6
29
1.2
2.0
97.1
143.00
213.00
32.86
315.34
469.71
190.15
283.23
.03332-/
4?
6
12-05-75
.600
40.0
29.25
.412
13.89
68.3
.39
154.8
.21
35.0
.650
17,2
9.2
4.1
69.5
31.12
26.53
.850
.006
73.2
8
-0.00
29.25
91.5
29
.9
1.7
106.8
69.00
105.00
34.29
178.32
271.35
96.30
146.55
.00982k/
.01494k/
64
  al  x 10-3.
  b_/  Per stack; to obtain total for kiln, multiply by 8.
                                  141

-------
                           TABLE D-27  (Concluded)
NAME      DESCRIPTION

       DATE OF HUN

DN     PROBE TIP DIAMETER
TT     NET TIME OF RUN
PB     BAROMETRIC PRESSURE
PM     AVG ORIFICE PRE5 DROP
VM     VOL DRY GAS-METER COND
TM     AVG GAS METER TEMP
VMSTM  VOL DRY GAS-STD COND
VW     TOTAL H20 COLLECTED
VWM    VOL H20 VAPOR-5TD COND
PMOS   PERCENT MOISTURE BY VOL
MD     MOLE FRACTION DRY GAS
PC02   PERCENT C02 BY VOL« DRY
P02    PERCENT 02 BY VOL, DRY
PCO    PERCENT CO BY VOL« DRY
PN2    PERCENT N2 BY VOL» DRY
MWD    MOLECULAR WT-DRY STK GAS
MW     MOLECULAR WT-STK GAS
CP     PITOT TUBE COEFFICIENT
DPS    AVG STK VELOCITY HEAD
TSM    AVG STACK TEMPERATURE
NP     NET SAMPLING POINTS
PST    STATIC PRES OF STACK
PS     STACK PRESSURE* ABSOLUTE
VSM    AVG STACK GAS VELOCITY
AS     STACK AHEA
QSM    STK FLOWRATE* DRY,STD CN
QAM    ACTUAL STACK FLOWRATE
PERI   PERCENT 1SOKINETIC     ,
MF     PARTICULAR WT-PARTIAL-
MT     PARTICULATE WT-TOTAL-
IC     PERC IMPINGER CATCH   /
CANM   PART. LOAD-PTL»STD CN-/
CAOM   PART. LOAO-TTL.STD CN~/
CATM   PART. LOAD-PTL*STK CN^/
CAUM   PART. LOAO-TTL.STK CN""
CAWM   PARTIC EMIS-PARTIAll-7
CAXM   PARTIC EMIS-TOTAll-'
EA     PERCENT EXCESS AIR
                                  UNITS
                                     IN
                                    MIN
                                  IN.HG
                                 IN.H20
                                    DCF
                                  DEG.F
                                    NCM
                                     ML
                                    NM3
                                 IN.H20
                                  DEG.C

                                  IN.HG
                                  IN.HG
                                  M/MIN
                                    IN2
                                 NM3/MIN
                                 M3/MIN

                                     MG
                                     MG

                                 MR/NM3
                                 MG/NM3
                                  MG/M3
                                  MG/M3
                                  KG/HR
                                  KG/HR
12-06-75

    .600
    35.0
   29.65
    .357
   10.99
    45.3
     .3?
    96.1
     .13
    28.5
    ,715
    16.1
     6.4
     1.5
    76.0
   30.H3
   27.18
    .850
    .006
    68.3
       7
   -0.00
   29.65
    87.1
      29
     1.0
     1.6
    95,0
    0.00
  191.00
  100.00
    0.00
  588.70
    0.00
  359.52
 0.00000.
                                                39
10
12-07-75
.600
40.0
29.65
.312
11.98
44,3
.35
168.0
.23
38.9
.611
18.2
5.1
5.5
71.2
31.12
26.01
.850
.005
95.8
8
-0,00
29.65
89.6
29
.8
1.7
111.8
160.00
416.00
61.54
451.57
1174.09
217.97
566.73
.02176S/
.05657£/
14
12
12-03-75
.600
35.0
29.35
,193
7.99
44.2
.23
83.0
.11
32.3
.677
22.3
1.1
6.7
69.9
31.61
27.21
.850
.003
125.9
7
-0.00
29.35
74.0
29
.7
1.4
100.5
448.00
795.00
43.65
1915.38
3398.95
938,08
1664.67
.07741-7'
.13738b-/
-11
a/  x 10-3.
b/  Per stack; to obtain total for kiln, multiply by 7.
£/  Per stack; to obtain total for kiln, multiply by 8.
                                  142

-------
                                                 TABLE D-28
                                    SUMMARY OF RESULTS (POM-LIKE^ MATERIAL )
CO
              NAME      DESCRIPTION

                     DATE  OF  RUN
UNITS       346

         13-03-75   12-04-75   12-05-75
VMSTD VOL DRY GAS-STD CONO DSCF
PMOS PERCENT MOISTURE BY VOL
TS AVG STACK TEMPERATURE DEO.F
OS STK FLOwRATE. DRYtSTD CN DSCFM
OA ACTUAL STACK FLOWRATE ACFM
PERI
PART
MF
CAN
CAT
CAW
PART
MT
CAO
CAU
CAX
1C
PERCENT ISOKINETIC
ICULATE
PART
PART
PART
PART
S
I
•
•
I
ICULATES
PART
PART
PART
PART
PERC
I
•
•
I

— PARTIAL CATCH
CULATE NT-PARTIAIr/
LOAD-PTL.STD CN-}
LOAO-PTL»STK CN-7
C FMIS-PARTIAt^'
— TOTAL CATCH
CULATE WT-TOTAlr^/.
LOAD-TTL»STD CN~/
LOAO-TTL,STK CN~
C F.MIS-TOTAL-
IMPINGER CATCH

MG
GR/DSCF
GR/ACF
LB/HR

MG
GR/DSCF
GR/ACF
LB/HR

DSCF

OEO.F
DSCFM
ACFM

15.64
25.0
150.0
42
67
93.5
15.98
28.5
155.6
42
69
97.1
13.64
35.0
163.8
32
60
106. B
MG
GR/DSCF
GR/ACF
LB/HR
345.00
.33970
.21694
.12366k/
143.00
.13781
.08309
.04932k/
69.00
.07792
.04208
.02164k/
                                                             376.00
                                                             .37022
                                                             .23643
                                                             .13477k/
                                                               8.24
                      213.00
                      .20526
                      •12377
                      .073472/
                       32.86
              a/  x 10-3.
              b/  Per stack; to obtain total for kiln, multiply by 8.
105.00
.11858
.06404
,03294k/
 34.29

-------
                             TABLE D-28  (Concluded)
NAME       DESCRIPTION

        DATE OF  RUN
             12
UNITS       fl          10

         12-06-75   12-07-75   12-08-75
VMSTD
PMOS
TS
QS
QA
PERI
PARTI

MF
CAN
CAT
CAW
PARTI
MT
CAO
CAU
CAX
1C
VOL DRY GAS-STD COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATF. » DRY,STD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
CULATES — MARTIAL CATCH
a/
PARTICULATE NT-PARTIAL",
a /
PART. LOAO-PTL.STD CN|/
PART. LOAD-PTL»STK CN-
PARTIC E.MIS-PARTIAL-
CULATES — TOTAL CATCH
PARTICULATE WT-TOTAL^ /
PART. LOAD-TTL»STD CN-/
PART. LOAU-TTL.STK CN~
PARTIC EMIS-TOTAL-'
PERC IMPINGER CATCH
DSCF

DEG.F
OSCFM
ACFM



MG
GR/DSCF
GR/ACF
Lfl/HR

MG
GR/DSCF
GR/ACF
LB/HR

DSCF

DEG.F
OSCFM
ACFM

11.43
Z8.5
155.0
35
57
95.0
12.49
38.9
204.4
28
59
111.8
8.24
3?. 3
258.6
24
49
100.5
MG
GR/DSCF
GR/ACF
Lfl/HR
0.00
0.00000
0.00000
0.00000
160.00
.19734
.09525
.04797k/
448.00
.83702
.40994
.17067£/
                                               191.00
                                               .25726
                                               .15711
                                               .07695£/
                                               100.00
416.00
.51308
.24766
.12472k/
 61.54
a/  x 10-TT
b/  Per stack;  to obtain total for kiln, multiply by 8.
£/  Per stack;  to obtain total for kiln, multiply by 7.
                                 795.00
                                1.48533
                                 .72746
                                 .30286£/
                                  43.65

-------
                                                    TABLE D-29
                                SUMMARY OF RESULTS—METRIC  UNITS  (POM-LIKE MATERIAL)
-p-
Ul
NAME        DESCRIPTION


        DATE OF RUN
                                                      UNITS
VMSTM VOL DRY GAS-STD COND
PMOS
TSM
QSM
0AM
PERI
EA
PART

MF
CANM
CATM
CAWM
PART
MT
CAOM
CAUM
CAXM
1C
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOWRATE, ORYtSTD CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PERCENT EXCESS AIR
ICULATES — PARTIAL CATCH
a/
PARTICULATE WT-PARTIAL-;
o /
PART. LOAD-PTL»STD CN-,
PART. LOAD-PTL«STK CN-
PARTIC EMIS-PARTIAL-
ICULATE.S — TUTAL CATCH
PARTICULATF WT-TOTA^ /
PART. LOAD-TTL.STD CN~/
PART. LOAO-TTLtSTK, CN~
PARTIC EMIS-TOTAL-
PERC IMPINRER CATCH
NCM

DEG.C
NM3/MIN
M3/MIN




'MG
MG/NM3
MG/M3
KG/HR

MG
MG/NM3
MG/M3
KG/HR

2
12-03-75
.443
25.0
65.5
1.2
1.9
93.5
67
345.00
777.34
496.43
.05 609^'
376.00
847.19
541.04
C\£L 1 1 *3 D /
• wO 1. J. J j
8.24
4
12-04-75
.453
28.5
68.7
1.2
2.0
97.1
A2
143.00
315.34
190.15
.02237-
213.00
469.71
283.23
.03332k/
32.86
6
12-05-75
,3«6
35.0
73.2
.9
1.7
106.8
64
69.00
17R.32
96.30
,00982^/
105.00
271.35
146.55
.01494^L/
34.29
                aj  x 10-3.

                b/  Per stack; to obtain total for kiln,  multiply by 8.

-------
                             TABLE D-29  (Concluded)
NAME
           DESCRIPTION
UNITS
        DATE OF
VMSTM
PMOS
TSM
QSM
0AM
PERI
EA
PARTI

MF
CANM
CATM
CAWM
PARTI

MT
CAOM
CAUM
CAXM
1C
VOL DHY OAS-STO COND
PERCENT MOISTURE BY VOL
AVG STACK TEMPERATURE
STK FLOrtRATE, DRYtSTO CN
ACTUAL STACK FLOWRATE
PERCENT ISOKINETIC
PERCENT EXCESS AIR
CULATES — PARTIAL CATCH
a/
PARTICULAR WT-PARTIAlr,
a /
PART. LOAD-PTL»STO CNF7,
PART. LOAO-PTLtSTK CN-
PARTIC EMIS-PARTIAL-
CULATES — TOTAL CATCH
a/
PARTICULATE WT-T()TAL~ a/
PART. LOAO-TTL»STD CN~/
PART. LOAD-TTL»STK, CN~
PART1C EMIS-TOTAL-'
PERC IHPIN6ER CATCH
MCM

OEG.C
NM3/MIN
M3/MIN




MG
MG/NM3
MG/M3
KG/HR


MG
MR/NM3
MG/M3
KG/HR

0
12-06-75
.324
28.5
68.3
1.0
1.6
95.0
39
0.00
0.00
0.00
0.00000
191.00
588.70
.0349l£/
100.00
10
12-07-75
.354
38.9
95.8
.8
1.7
111.8
14
160.00
451.57
217.97
416.00
1174.09
566.73
.05657^
61.54
12
12-08-75
.233
3?. 3
125.9
.7
1.4
100.5
-11
440.00
1915.38
938.08
.0774l£/
795.00
3398.95
1664.67
.13738£/
43.65
bf  Per stack; to obtain total  for kiln, multiply  by  8.
£/  Per stack; to obtain total  for kiln, multiply  by  7.

-------
           APPENDIX E
FLUE GAS COMBUSTION COMPUTATIONS
              147

-------
          The computations that follow are based on  data  found in the

Handbook of Chemistry and Physics,  23rd Edition—  and Lange's Handbook

of Chemistry"  and assumptions made as noted.

          A long chain aliphatic hydrocarbon,  Bryonane (C-nH,  , mol wt

282), has been taken to represent the tar and  oil fraction of  the flue

gas stream. A mole of any referenced gas is assumed  to occupy  0.79 cu

ft. A theoretical flame temperature of 3790°F  (2090°C) based on several

natural gas streams—  was used for combustion  of the flue gas  stream.

This natural gas then requires 16 cu ft air per cubic foot natural gas-

in addition to that required for combustion of the flue gas  stream, and

will produce 24,500 cal/cu ft natural gas.

          Heats of vaporization of water are as follows:—4—

         Temperature (°C)        Heat of vaporization (cal/g)

                60                          563.2
                70                          557.5
                95                          542.7
               145                          507.3

          Specific heats of the various compounds are as  follows:—

             Compound             Specific heat (cal/g/°C)

          Air                               0.24
          Carbon dioxide                    0.20
          Carbon monoxide                   0.25
          Nitrogen                          0.25
          Oxygen                            0.22
          Water                             0.48
                                 148

-------
          Computations to determine the net heat available from the flue

gas stream are based on the heats of combustion of the water and tar and

oil fractions less the heat of vaporization of the water.

          Computations to determine the air fuel ratio (amount of air to

be added per amount of flue gas to allow combustion) are based on stoi-

chiometric combustion of the given amount of C nH,  available in each

s'ample.

          Calculations to determine the amount of natural gas needed for

combustion of the flue gas are based on raising the gas stream and addi-

tional air from the stack temperature to the flame temperature. For the

water fraction this includes the heat of vaporization.

          These values must be taken as approximate or "ball-park" esti-

mates. The positive heat of combustion for the water fraction indicates

the presence of entrained volatile organics. The tar and oil fraction is

composed of many constituents which may not be accurately represented by

C  H  • Some constituents may have passed through the sampling train with-

out entrapment or have been lost during sample recovery. Any or all of

these factors may contribute to errors in the calculations.

December 4

          Net heat available from flue gas stream:

            Water fraction:  (296 cal/g) (8.4 g) = 2,486.4 cal
                             (-557.5 cal/g) (8.4 g) = -4,683.0 cal
                                  149

-------
  Tar and oil fraction:  (1,185 cal/g) (0.6 g) = 711.0 cal

    Net      2,486.4 cal
          +    711.0 cal
             3,197.4 cal
            -4,683.0 cal
            -1,485.6 cal

Air/fuel ratio:

  0.6 g C QH   (mol wt 282) = 0.002 mole

H20
C02

02
CO
No
% by Volume
30.5
15
(of 69.5)
7.3
2.9
74.8
Volume (cu ft)
0.2562
0.08757

0.0426174
0.0169302
0.4366824
Moles
0.47
0.11

0.05
0.02
0.55
                            0.84
0.002
                 0.061
0.04 CO  + 0.042 HO
  0.061 mole 0  required
  0.05  mole 0  available in flue gas
  0.011 mole 0« additional required
   0.011 mole 0,
  0.002 mole fuel
                   = 5.5
  mole air  _ volume air
  mole fuel   volume fuel
                        = air/fuel ratio = (5.5)1
                  .1 J
                 0.21;
  Requires 26.2 cu ft air to combust 1 cu ft flue gas

Flue gas combustion:
= 26.2
  Stack temperature = 70 C
                               AT = 2090°C - 70°C  = 2020°C
                        150

-------
Constituent
Moles
Specific heat
  (cal/g/°C)
Heat required
  per volume
  stack gas
sampled (cal)
Heat required
  per cu ft
  stack gas
    (cal)
C02
02
CO
N2
H20

Combustion
0.11
0.05
0.02
0.55
0.47
(100°C to
0.05
0.20
0.22
0.25
0.25
0.48
2090°C = AT = 1990°C)
0.24
1,955
711
283
7,777
8,801

698
2,328
846
337
9,258
9.620
22,389
831
  air
Heat of
  vaporization
                              4,683

                       Heat required

     Water fraction           2,486
     Tar and oil fraction       711

                       Net heat available
                       Net heat required
                                     5,575

                                    28,795

                                     2,690
                                       846

                                     3,806
                                    24,989
            Thus, 1.02 cu ft natural gas required per cubic foot flue
              gas and approximately 42 cu ft air total
December 6
          Net heat available:

            Water fraction:  (227 cal/g) (4.6 g) = 1,044.2 cal
                             (-557.5 cal/g) (4.6 g) = 2,564.5 cal

            Tar and oil fraction:  (7,256 cal/g) (0.6 g) = 4,353.6 cal

              Net:  +2,833.3 cal

          Air/fuel ratio:

            0.002 mole
            0.05  mole 02
                                  151

-------
            0.002  CnftH,  + 0.061  On	>  0.04 CO., + 0.042 H.O
                   20  42           2                 2           2.
            0.011 mole 0   required
             0.011 mole 0,
            0.002 mole fuel
            Air/fuel ratio = -r~— = 26.2
                            u »i i
          Flue gas  combustion:
      Constituent
Moles
        ization
Specific heat
  (cal/g/°C)
                               Heat required
Heat required
  per cu ft
  stack gas
    (cal)
C02
02
CO
N2
H20

Combustion air
Heat of vapor-
0.13
0.05
0.01
0.63
0.26

0.05

0.20
0.22
0.25
0.25
0.48

0.24

2,458
756
150
9,477
4.756
17,597
743
2,728
                                21,068
                        Water fraction
                        Tar and oil fraction
                                 1,111
                                 4,631
                               Net heat available       5,742
                               Net heat required       15,326

            Requires 0.63 cu ft natural gas per cubic foot flue gas and
              approximately 36 cu ft air total
December 7
          Net heat available:

            Water fraction:  (153 cal/g) (16.3 g) = 2,493.9 cal
                             (-542.7 cal/g) (16.3 g) = -8,846.01 cal
                                 152

-------
      Tar and oil fraction:   (7,097 cal/g) (1.2  g)  = 8,516.4 cal

        Net:  +2,164.3 cal

    Air/fuel ratio:
      0.004 mole G  H
      0.08 mole 0
0.004
                     0.122
          0.08 CO  + 0.084 HO
      0.042 mole 0  required
       0.042 mole 0,
      0.004 mole fuel
                       = 10.5
      Air/fuel ratio = 50
    Flue gas combustion:
Constituent
           Moles
Specific heat
  (cal/g/°C)
  ization
                          Heat required

                   Water fraction
                   Tar and oil fraction
Heat required
  per cu ft
  stack gas
    (cal)
C02
02
CO
N2
H20

Combustion air
Heat of vapor-
0.30
.0.08
0.09
1.16
0.91

0.20

0.20
0.22
0.25
0.25
0.48

0.24

2,801
598
669
8,617
8,322
21,007
1,467
4.705
                                           27,179

                                            1,326
                                            4,530
                          Net heat available      5,856
                          Net heat required      21,323
                           153

-------
            Requires 0.87 cu ft natural gas per cubic foot flue gas and
              approximately 64 cu ft air total
December 8 - First Run
          Net heat available:

            Water fraction:  (173 cal/g) (11.0 g) = 1,903 cal
                             (-507.3 cal/g) (11.0 g) = -5,580.3 cal

            Tar and oil fraction:  (8,877 cal/g) (0.6 g) = 5,326.2 cal

              Net:  +1,648.9 cal

          Air/fuel ratio:
            0.002 mole C QH
            0.02  mole Q
            0.002 G  H   + 0.061 0 	>  0.04 CO  + 0.042 H20
            0.041 mole 0  required
             0.041 mole 0,
            0.002 mole fuel
                             = 20.5
            Air/fuel ratio = 97.6
                                  154

-------
          Flue gas combustion:
      Constituent
Moles
Specific heat
  (cal/8/°C)
Heat required
  per cu ft
  stack gas
    (cal)
C02
02
CO
N2
H20

Combustion air
Heat of vapor-
0.48
0.02
0.15
1.52
0.61

0.20

0.20
0.22
0.25
0.25
0.48

0.24

3,197
107
795
8,052
4,801
16,232
1,046
2,171
        ization
                                Heat required          19,449

                         Water fraction                   740
                         Tar and oil fraction           2,072

                                Net heat available      2,812
                                Net heat required      16,637

            Requires 0.68 cu ft natural gas per cubic foot flue gas and
              approximately 109 cu ft air total
                /
December 8 - Second Test

          Net heat available:

            Water fraction:  (855 cal/g) (11.8 g) = 10,089 cal
                             (-507.3 cal/g) (11.8 g) = -5,986.14 cal

            Tar and oil fraction:  (4,715 cal/g) (0.6 g) = 2,829 cal

              Net:  +6,931.9 cal

          Air/fuel ratio:

            0.002 mole C 0H,
            0.02  mole 0
                                  155

-------
      0.002 C  H   + 0.061 0
                     0.04 CO  + 0.042 HO
      0.041 mole 0  required
       0.041 mole 0,
      0.002 mole fuel
                       = 20.5
      Air/fuel ratio = 97.6
    Flue gas combustion:
Constituent
Moles
  ization
Specific heat
  (cal/g/°C)
                          Heat required
Heat required
  per cu ft
  stack gas
    (cal)
C02
02
CO
N2
H20

Combustion air
Heat of vapor-
0.48
0.02
0.14
1.49
0.66

0.20

0.20
0.22
0.25
0.25
0.48

0.24

3,260
109
756
8,050
4,503
16,678
2,134
2,375
                                21,187
                   Water fraction
                   Tar and oil fraction
                                 4,004
                                 1,123
                          Net heat available      5,127
                          Net heat required      16,060

      Requires 0.66 cu ft natural gas per cubic foot flue gas and
        approximately 108 cu ft air total
                            156

-------
        APPENDIX F
COMPUTATION OF KILN VOLUME
           157

-------
 All units in inches
 unless otherwise
 noted
Area A:
   a = 84
   b=60
   c = 60
Area A = 233.576 sq in.
        = 1.622  sq ft
                                    =/(a)2  + (b + c)2 = N/(84)2 + (120)2

                                         = 146.4786674
                               a + f = 126
                                   f = 126 - 84 = 42
                                  R2 = /(a +  f)2 +  (c)2 =/(126)2 +  (60)2

                                         = 139.5564402

                                       Ri 4. Ro
                                     _   L -r    = 143.0175538
                                           /2      2   /    2       2
                                        (b)  + (f)  =V(60)^ + («r

                                         = 73.23933369
                                     = 1/2
                                                      -  (d)  = 1/2
                                              (143)2  -  (73)2 = 138.2498488
                                   9=2  arc  sin
                                                  (2)


                                         = 2 arc sin  •
                                                           73    1
                                                       (2)  (143)J
                                   9  = 0.5178678409 radians
    si = (Ri
     1     1-^    i
           = 74.0641918


Area A = 1/2
       = 1/2 [(143) (74)
           = 233.5763633
                                                            (0'518) =
                                                               (e)]
                                                       -  (73)  (138)]
                                    158

-------
                                           R
Area B:
       S2
    a4f = 126
     c = 60
     R3 = 138
     R2 = 139.5564402
Area B = 139.622 sq in,
       = 0.970 sq ft
                                     2-3
                 = 138'7782201
     g = R3 - (a + f) = 138 - (126) = 12
                                       h = Vg2 + c2 =/12)2 + (60)2
                                             = 61.18823416
                                       i = 1/2 \/4(R2_3)2 - (h)2
                                                     ) (139) - (61)
                                             = 135.3639331
                                                                   2
                                      9=2 arc sin
                                                      (2)
          = 2  arc sin
                       (2)  (139)
    9  = 0.4445583706 radians

    S2 = (R2_3) (62) = (139) (0.445)

           = 61.69501066

Area B = 1/2 [(R2_3> (S^ - (h) (i)]


       = 1/2 [(139) (62) - (61) (135)]
           = 139.6218666
Area C:
                                  Area G = 1/2 (b) (f) = 1/2 (60) (42)

                                         = 1,260

                                  Area C = 1,260 sq in.


                                         = 8.75 sq ft
     b = 60
     f =42
                                   159

-------
Area D:
  c = 60
  f = 42
    = 54
                f+g
    Area D = 1/2 [(f) + (f + g)] c
               = 1/2 [42 + 54] 60

           = 2,880

    Area D = 2,880 sq in.

           = 20 sq ft
Area E and F:
Area E and F =
    a = 84
    b = 60
    c = 60
Area of Kiln End:
              (a) (b + c) = (84) (120)
                = 10,080
                                Area E and F = 10,080  sq  in,

                                            = 70  sq ft
Total Area =(A
                                    F)x2
                                           =  233.576 + 139.622 + 1,260
                                               + 2,280 + 10,080

                                           =  14,693.198 sq in.

                                           =  (101.342 sq ft) x 2

                                           =  202.683 sq ft
                                 160

-------
Volume of kiln:                 Volume = (area) x (length)

                                       = (202.683) (32)

                                       = 6,485.866 cu ft (183.659 cu m)

          As one cord of wood is 4 ft x 4 ft x 8 ft, the volume of one
cord of wood is 128 cu ft (3.625 cu m). Thus, the volume of the kiln is
approximately 50.67 cords.

          Allowing for air space left along the walls and roof and pro-
vided along the floor, the total amount of wood in the kiln would be
approximately 45 cords.
                                   161

-------
         APPENDIX G
PRELIMINARY RUNS - FIELD DATA
             162

-------
                                              TABLE G-l
                                  PRELIMINARY DATA AND CALCULATED VALUES
                                  RUN-   1-P    DATE- 09-29-75
OJ
         ATMOS   ATMOS   STACK    H20
         TEMP    PRES     VAC   COND
        (DG.F)  (I.HG)  (I.H20)  (ML)
         70.0    29.15
  0.00
42.9
PARTIC   PARTIC  STACK   INIT    PERC PERC PERC PITOT
WT-PTL   WT-TTL   AREA    VOL     02    C02  CO   TUBE
 (MG)     (MO)   (FT2)   (OCF)    DRY  DRY  DRY  COEF

   0.00     0.00     .20   548.70   3.0 13.0  3.5  .B50
PORT-
POINT

1
1
1
1
1
1

1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF)
549.86
551.02
552.17
553.34
554.60
556,56
        DELTA   DELTA  TEMP  TEMP TRAIN   STACK  S.GEL  PROBE
          P       H     IN    OUT  VAC     TEMP   TEMP  T DIA   VEL
(DCF)  (I.H20) (I.H20) (D.F)  (D.F) (I.HG)  (D.F)  (D.F)  (IN)    (FPM)
                               .004
                               .004
                               .004
                               .004
                               .004
                               .004
                  135
                  135
                  135
                  135
                  135
                  200
              69.0
              70.0
              75.0
              79.0
              81.0
              83.0
             7040
             70.0
             70.0
             72.0
             74.0
             75.0
2.0
2.0
2.0
2.0
2*0
2.5
190.0
190.0
240.0
200.0
200.0
200.0
60.0
.597  250.0
.597  250.0
.597  250.0
.597  250.0
.597  250.0
.597  250.0

-------
                                       TABLE G-2
                           PRELIMINARY DATA AND CALCULATED VALUES
                          RUN-
                   2-p
DATE- 09-29-76
 ATMOS  ATMOS  STACK   HHO    PARTIC
 TEMP   PRES    VAC   COND    WT-PTL
(DG.F) (I.HG) (I.H20) (ML)     (MG)

 70.0   29.12   0.00   35.0     0.00
                         PARTIC   STACK   INIT
                         WT-TTL    AREA    VOL
                           (MG)    (FT?)   (DCF)
                      PERC PERC PERC PITOT
                       02    C02  CO   TUBE
                       DRY  DRY  DRY  COEF
                            0.00
          .20  556.56   3.0 13,0  3.5  .850
 PORT-  SAMP
 POINT  TIME
       (MIN)
METER   DELTA   DELTA  TEMP   TEMP  TRAIN  STACK S.GEL PROBE
 VQl       P       H      IN     OUT   VAC    TEMP  TEMP T DIA    VEL
(DCF) (I.H20)  (I.H20)  (D.F)  (D.F)  (I.HG)  (D.F) (D.F) (IN)    (FPM)

                                                       .594   250.0
                                                       .594   250.0
                                                       .594   250.0
                                                 75.0  ,594   250.0
                                                       ,594   250.0
                                                       ,594   250.0
1
1
1
1
1
1
1
1
1
1
1
1
5.00
5.00
5.00
5.00
5.00
5.00
557.24
558,61
560.03
561.40
562.70
563.95
.004
.004
.004
.004
.004
.004
.170
.210
.210
.200
.170
.170
75.0
78.0
84.0
87.0
89.0
90.0
76.0
77.0
78.0
80.0
81.0
82.0
2.0
2.0
2.0
2.0
2.0
2.0
230.0
230.0
200.0
200.0
200.0
290,0

-------
                                               TABLE G-3
                                   PRELIMINARY DATA AND CALCULATED VALUES
                                   RUN-   3-P
                         DATE- 11-04-75
01
         ATMOS  ATMOS  STACK    H20
         TEMP   PRES    VAC    COND
        (DG.F) (I.HG)  (I.H20)  (ML)
         65.0   29.38
0.00
47.0
PARTIC
WT-PTL
(MG)
0.00
PARTIC
WT-TTL
(MG)
0.00
STACK
AREA
(FT2)
.20
INIT
VOL
(DCF)
232.3
PERC PERC  PERC PITOT
 02   C02   CO   TUBE
 DRY  DRY   DRY  COEF

  .5 20.0   4.7  .850
PORT-
POINT

1
1
1
1
1
1

1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5,00
5.00
5.00
5,00
METER
VOL
(DCF) (
233.70
234.59
235.12
236.27
237.36
230.26
DELTA
P
I.H20)
.003
.003
.003
.003
.003
.003
DELTA
H
(I.H20)
.170
.170
.170
.170
.170
.170
TEMP
IN
(D.F)
68.0
71.0
73.0
75.0-
78.0
80.0
TEMP
OUT

-------
                                                TABLE G-4
                                    PRELIMINARY DATA AND CALCULATED VALUES
                                   RUN-
                  4-P
                  DATE- 11-04-75
CTi
         ATMOS  ATMOS  STACK    H20
         TEMP   PRES    VAC    COND
        (06.F) (I.HG)  (I.H20)  
         75.0   29.34
0.00
PARTIC
WT-PTL
(MG)
-PARTIC
WT-TTL
(MG)
STACK
AREA
(FT?)
INIT
VOL
(DCF)
46.5
0.00
0.00
                                               PERC PERC  PERC PITOT
                                                0?   C02   CO   TUBE
                                                DRY  DRY   DRY  COEF
.20  238.26    .5  20.0  4.7  .850
PORT-
POINT

1
1
1
1
1
1

1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
239.33
240.28
241.03
241.63
242.30
243.20
DELTA
P
I.H20)
• 003
.003
.003
.003
.003
.003
DELTA
H
(I.H20)
.050
.050
.050
.050
.050
.050
TEMP
IN

-------
                                       TABLE G-5
                           PRELIMINARY DATA AND CALCULATED VALUES
                          RUN-    5-P
 DATE- 11-04-75
 ATMOS  ATMOS  STACK   H20     PARTIC
 TEMP   PRES    VAC   COND     WT-PTL
(DG.F) (I.HG) (1.H20) (ML)      (MG)

 75.0   29.34   0.00   86.5      0.00
PARTIC  STACK   INIT
WT-TTL   AREA    VOL
 (MG) "  (FT2)   (DCF)
            PERC  PERC PERC PITOT
             OH    C02  CO   TUBE
             DRY   DRY  DRY  COEF
  0.00
.20  243.20    .5  20,0  4.7
,850
PORT-
POINT

1
1
1
1
1
1

1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
244.31
245.36
246.33
247.40
248.49
249.55
DELTA
P
I.H20)
.002
.002
.002
.002
.002
.002
DELTA
H
(I.H20)
.130
.120
.120
.120
.170
.150
TEMP
IN
(D.F)
82.0
82.0
82.0
84.0
84.0
84.0
TEMP
OUT
(D.F)
81.0
82.0
82.0
82.0
82.0
82.0
TRAIN
VAC
(I.MG)
2.0
2.5
3.0
5.0
7.0
6.0
STACK
TEMP
(D.F)
245.0
270.0
270.0
270.0
270.0
270.0
S.GEL PROBE
TEMP T DIA
(O.F) (IN)
.613
.613
.613
65.0 .613
.613
.613

VEL
(FPM)
200.0
200.0
200.0
200.0
200.0
200.0

-------
                                               TABLE G-6
                                   PRELIMINARY DATA AND CALCULATED VALUES
                                   RUN-
6-P
DATE- 11-04-75
Ov
oo
         ATMOS  ATMOS  STACK    HHO    PARTIC   PARTIC
         TEMP   PRES    VAC    CONO    WT-PTL   WT-TTL
        (06.F) (I.H6)  (I.H20)  (ML)      (M6)     (MG)

         75.0   29.35   0.00    64.0     0.00      0.00
               STACK  INIT   PERC PERC  PERC PITOT
                AREA   VOL    02   C02   CO   TUBE
               (FTH)  (DCF)   DRY  DRY   DRY  COEF

                 .20  249.55   .5 20.0   4.7  .850
PORT-
POINT

1
1
1
1
1
1

1
1
1
1
1
1
SAMP
TIME
(MIN)
5.00
5.00
5.00
5.00
5.00
5.00
METER
VOL
(DCF) (
250.50
251.35
252.50
253.70
254.74
255.75
DELTA
P
I.H20)
.002
.002
.002
.002
.002
.002
DELTA
H
(I.H20)
.130
• 130
.150
.170
.150
.150
TEMP
IN
(D.F)
78.0
78.0
78.0
80.0
83.0
86.0
TEMP
OUT
(D.F)
78.0
78.0
79.0
79.0
80.0
80.0
TRAIN
VAC
(I.HG)
7.5
8.0
7.5
. 6.0
6.5
6.5
STACK S.GEL
TEMP TEMP
(D.F) (D.F)
270.0
280.0
280.0
280.0
280.0
280.0
PROBE
T DIA
(IN)
.613
• 613
.613
.613
.613
.613

VEL
(FPM)
200.0
200.0
200.0
200.0
200.0
200.0

-------
                                             TABLE G-7
                                       PRELIMINARY EMISSION DATA
cr>
NAME      DESCRIPTION            UNITS      1-P

       DATE OF RUN                       09-39-75

DN     PROBE TIP DIAMETER           IN        .597
TT     NET TIME OF RUN             MIN        30.0
PB     BAROMETRIC PRESSURE       IN.HG      29.15
PM     AVG ORIFICE PRES DROP    IN.H20        .146
VM     VOL DRY GAS-METER COND      DCF        7.86
TM     AVG GAS METER TEMP        DEG.F        74*0
VMSTD  VOL DRY GAS-STD COND       DSCF        7.60
VW     TOTAL H20 COLLECTED          ML        43,9
VWV    VOL H20 VAPOR-STD COND      SCF        2.03
PMOS   PERCENT MOISTURE BY VOL                21.1
MD     MOLE FRACTION DRY GAS                  .789
PC02   PERCENT C02 BY VOL, DRY                13,0
P02    PERCENT 02 BY VOL, DRY                 3.0
PCO    PERCENT CO BY VOL, DRY                 3.5
PN2    PERCENT N2 BY VOL, DRY                 80.5
MWD    MOLECULAR WT-DRY STK GAS             30.20
MW     MOLECULAR WT-STK GAS                 27.63
CP     PITOT TUBE COEFFICIENT                 .850
DPS    AVG STK VELOCITY HEAD-   IN.H20        .004
TS     AVG STACK TEMPERATURE     DEG.F      203.3
NP     NET SAMPLING POINTS                       6
PST    STATIC PRES OF STACK      IN.HG      -0,00
PS     STACK PRESSURE, ABSOLUTE  IN.HG      29.15
VS     AVG STACK GAS VELOCITY      FPM        250
AS     STACK AREA                  IN2         29
OS     STK FLOWRATE, DRY,STD CN  DSCFM         31
QA     ACTUAL STACK FLOWRATE      ACFM         50
PERI   PERCENT ISOKINETIC                     84.6
EA     PERCENT EXCESS AIR                        6
2-P
09-29-76
.594
30.0
29.12
.188
7.39
61.4
7.04
35,0
1.66
19.1
.809
13.0
3.0
3.5
80,5
30.20
27.87
.850
.004
225.0
6
-0.00
29.12
250
29
30
50
79.8
6
3-P
11-04-75
.592
30.0
29,38
.170
5.87
71,8
5.75
47.0
2.23
27.9
.721
20.0
.5
4.7
74.8
31.22
27.53
.850
.003
203.3
6
-0.00
29.38
222
29
25
44
79.7
-9

-------
                           TABLE G-7  (Concluded)
NAME      DESCRIPTION            UNITS

       DATE OF RUN

DN     PROBE TIP DIAMETER           IN
TT     NET TIME OF RUN             MIN
PB     BAROMETRIC PRESSURE       IN.HG
PM     AVG ORIFICE PRES DROP    IN.H20
VM     VOL DRY GAS-METER COND      DCF
TM     AVG GAS METER TEMP        DEO.F
VMSTD  VOL DRY GAS-STD COND       DSCF
VW     TOTAL H?0 COLLECTED          ML
VWV    VOL H20 VAPOR-STD COND      SCF
PMOS   PERCENT MOISTURE BY VOL
MD     MOLE FRACTION DRY GAS
PC02   PERCENT C02 BY VOL» DRY
P02    PERCENT 02 BY VOL» DRY
PCO    PERCENT CO BY VOL» DRY
PN2    PERCENT N2 BY VOLi DRY
MWD    MOLECULAR WT-DRY STK GAS
MW     MOLECULAR WT-STK GAS
CP     PITOT TUBE COEFFICIENT
DPS    AVG STK VELOCITY HEAD    IN.H20
TS     AVG STACK TEMPERATURE     DEG.F
NP     NET SAMPLING POINTS
PST    STATIC PRES OF STACK      IN.HG
PS     STACK PRESSUREt ABSOLUTE  IN.HG
VS     AVG STACK GAS VELOCITY      FPM
AS     STACK AREA                  IM2
OS     STK FLOWRATEt DRYtSTD CN  DSCFM
OA     ACTUAL STACK FLOWRATE      ACFM
PERI   PERCENT ISOKINETIC
EA     PERCENT EXCESS AIR
4-P
11-04-75
.613
30.0
29.34
.050
4.94
78.7
4.77
46.5
2.20
31.6
.684
20*0
.5
4.7
74.8
31.22
27.04
.850
.003
245.8
6
-0.00
29.34
220
29
22
44
69.8
-9
5-P
11-04-75
.613
30.0
29.34
.135
6.35
82,4
6.09
86.5
4.10
40.3
.597
20.0
.5
4.7
74.8
31.22
25.90
.850
.002
265.8
6
-0.00
29.34
200
29
17
40
115.3
-9
6-P
11-04-75
.613
30.0
29.35
.147
6.20
79.8
5.97
64.0
3.03
33.7
.663
20.0
.5
4.7
74.8
31.22
26.77
.850
.002
278.3
6
-0.00
29.35
200
29
19
40
103.7
-9

-------
                                 TABLE G-8
                   PRELIMINARY EMISSION DATA (METRIC RESULTS)
NAME      DESCRIPTION            UNITS

       DATE OF RUN

ON     PROBE TIP DIAMETER           IN
TT     NET TIME OF RUN             MIN
PB     BAROMETRIC PRESSURE       IN.HQ
PM     AV6 ORIFICE PRES DROP    IN.H20
VM     VOL DRY GAS-METER COND      DCF
TM     AV6 GAS METER TEMP        DEG.F
VMSTM  VOL DRY GAS-STD CONO        NCM
VW     TOTAL H20 COLLECTED          ML
VMM    VOL H20 VAPOR-STD COND      NM3
PMOS   PERCENT MOISTURE BY VOL
MD     MOLE FRACTION DRY GAS
PC02   PERCENT C02 BY VOL» DRY
P02    PERCENT 02 BY VOL» DRY
PCO    PERCENT CO BY VOL* DRY
PN2    PERCENT N2 BY VOL• DRY
MWD    MOLECULAR WT-DRY STK GAS
MW     MOLECULAR WT-STK GAS
CP     PITOT TUBE COEFFICIENT
DPS    AVG STK VELOCITY HEAD    IN.H20
TSM    AVG STACK TEMPERATURE     DEG.C
NP     NET SAMPLING POINTS
PST    STATIC PRES OF STACK      IN.HG
PS     STACK PRESSURE, ABSOLUTE  IN.HO
VSM    AVG STACK GAS VELOCITY    M/MIN
AS     STACK AREA                  IN2
QSM    STK FLOWRATEt DRYtSTD CN NM3/MIN
QAM    ACTUAL STACK FLOWRATE    M3/MIN
PERI   PERCENT ISOKINETIC
EA     PERCENT EXCESS AIR
1-p
09-29-75
.597
30.0
29.15
.146
7.86
74.0
.22
4?. 9
.06
21.1
.789
13.0
3.0
3.5
80.5
30.20
27.63
.850
.004
95.2
6
-0.00
29.15
76.2
29
.9
1.4
84.6
6
2-P
09-29-76
.594
30,0
29.12
.188
7.39
81.4
.20
35.0
.05
19.1
.809
13.0
3.0
3.5
80.5
30.20
27.87
.850
.004
107.2
6
-0.00
29.12
76.2
29
.9
1.4
79.8
6
3-P
11-04-75
.592
30.0
29.38
.170
5.87
71.8
.16
47.0
.06
27.9
,721
20.0
.5
4.7
74.8
31.22
27.53
.850
.003
95.2
6
-0.00
29.38
67.6
29
.7
1.3
79.7
-9

-------
                                        TABLE G-8  (Concluded)
NJ
NAME      DESCRIPTION            UNITS

       DATE OF RUN

DN     PROBE TIP DIAMETER           IN
TT     NET TIME OF RUN             MIN
PB     BAROMETRIC PRESSURE       IN.HO
PM     AV6 ORIFICE PRES DROP    IN.H20
VM     VOL DRY GAS-METER CQND      DCF
TM     AVG GAS METER TEMP        DEG.F
VMSTM  VOL DRY GAS-STD COND        NCM
VW     TOTAL H20 COLLECTED          ML
VMM    VOL H20 VAPOR-STD COND      NM3
PMOS   PERCENT MOISTURE BY VOL
MD     MOLE FRACTION DRY GAS
PC02   PERCENT C02 BY VOL» DRY
P02    PERCENT 02 BY VOLt DRY
PCO    PERCENT CO BY VOL. DRY
PN2    PERCENT N2 BY VOLt DRY
MWO    MOLECULAR WT-DRY STK GAS
MW     MOLECULAR WT-STK GAS
CP     PITOT TUBE COEFFICIENT
DPS    AVG STK VELOCITY HEAD    IN.H20
TSM    AVG STACK TEMPERATURE     DEG.C
NP     NET SAMPLING POINTS
PST    STATIC PRES OF STACK      IN.H6
PS     STACK PRESSURE, ABSOLUTE  IN.HG
VSM    AVG STACK GAS VELOCITY    M/MIN
AS     STACK AREA                  IN2
QSM    STK FLOWRATE. DRYtSTD CN NM3/MIN
QAM    ACTUAL STACK FLOWRATE    M3/MIN
PERI   PERCENT ISOKINETIC
EA     PERCENT EXCESS AIR
4-P»
11-04-75
.613
30.0
29.34
.050
4.94
78.7
.13
46.5
.06
31*6
.684
20.0
.5
4.7
74.8
31.22
27.04
,850
.003
118.8
6
-0.00
29.34
67.1
29
.6
1*2
69.8
-9
5-P
11-04-75
.613
30.0
29.34
.135
6.35
82.4
.17
86.5
.12
40.3
.597
20.0
.5
4.7
74.8
31.22
25.90
.850
.002
129.9
6
-0.00
29.34
61.0
29
.5
1*1
115.3
-9
6-P
11-04-75
.613
30.0
29.35
.147
6.20
79.8
.17
64.0
.09
33.7
.663
20.0
.5
4.7
74.8
31.22
26.77
.850
.002
136.8
6
-0.00
29.35
61.0
29
.5
1.1
103.7
-9

-------
             APPENDIX H
COMPUTATION FOR ISOKINETIC SAMPLING
                 173

-------
                                    a/
        (1.032) (TS + 460) (VMSTD)  -
         (VS) (TT) (PS) (MD) (DN)2
                            PM     ,
„.,--   (17.71) (VM) (PB + 13.6)  *
VMMD          (TM + 460)
        100 - PMOS  a/
           100
where:

     PERI = percent isokinetic sampling rate

     TS = stack temperature (°F)

     VMSTD = volume dry gas sampled,  standard conditions (dscf)

     VS = stack gas velocity (fpm)

     TT = net sampling time (rain)

     PS = stack pressure, absolute (in. Hg)

     MD = mole fraction, dry gas

     DN = probe tip diameter (in.)

     VM = volume dry gas sampled, meter conditions  (dcf)

     PB = barometric pressure (in. Hg)

     PM = orifice pressure drop (in.  HO)

     TM = meter temperature (°F)

     PMOS = percent stack gas moisture, by volume
a/  From Federal Register.—'
                          I/
                                 174

-------
                                              PM
PERI =
     - (I»Q32) (TS + 460) (17.71) (VM) (PB + 13.6)
          (VS) (TT) (PS) (MD) (DN)2 (TM + 460)
2~
(PERI) (TT) (DN)
(1,032) (17.71)
[(MD)]
(VS) (TM + 460)
(TS + 460)
     _ (PERI) (VS) (TT) (PS) (MD) (DN)  (TM + 460)
                                           PM       as  TT-T « PB;  PB ~ PS
         (1,032) (TS + 460) (17.71) (PB + 13.6)
  VM =
     Known for given test:

          PERI = 100

          TT = 5

          DN

     Known for given day:

          MD (based on preliminary or previous day)

     Known for each stack:

          VS

     Known for each 5-min sampling period:

          TM

          TS

          Thus for each incremental sampling period,  a  volume  to be  sam-

pled can be determined, approximating isolcinetic sampling  for each  per-

iod, stack, and run.
                                 175

-------
         APPENDIX I
TABLE OF METRIC EQUIVALENTS
             176

-------
       To convert  from

inch (in.)

foot (ft)

square inches (sq  in.)

square feet (sq ft)

cubic inches (cu in.)

cubic feet (cu ft)

pounds (lb)

pounds per cubic foot  (pcf)

degrees Fahrenheit (°F)


British Thermal Units  (BTU)

calories per gram  per  degrees
  centigrade (cal/g/°G)
                  To

centimeter (cm)

meter (m)

square meters (sq m)

square meters (sq m)

cubic meters (cu m)

cubic meters (cu m)

kilograms (kg)

kilograms per cubic meter (kg/ cu m)

degrees Gelsious (°C)


calories (cal)

joules per gram per degrees centigrade
  (joules/g/°C)
Multiply by

2.540 E-00

3.048 E-01

6.542 E-04

9.290 E-02

1.639 E-05

2.832 E-02

4.536 E-01

1.602 E+01

    t  - 32
2.52 E+02

4.185 E-00

-------