Columbus Incinerator
Waste-to-Energy Facility
Soil Sample Site Descriptions
Laboratory Analysis Data Sheets
U.S. Environmental Protection Agency
Region 5
Chicago, Illinois
April 1996
-------
Columbus Waste to Energy Facility
Soil Sampling Locations and Dioxln TEQ Concentrations
A/ rtiiuy Rood
A/ Cwntf Rood
A/ Nitftarhood Rood
/'/ JMP Troi
A/
A/ Pvwrid Stron
A/ Orah or Mvrrittat Slrton
/V Canty Bonkr
SoH
-------
Columbus Waste to Energy Facility
Sol Sampling Location* and Sampfe Numbers
*••••
Ti
A/
fa/ nirnvy Rood
A/Cwrty Rood
A/ N^/tertuod Rood
/V J**p 'nil
A/I
POMT TiuantMiai
Ptrcrid Slr«m
Drain or
Slrwn
So«S«nplngLoe«ton
VMM to Envgy Ftdfty
-------
ATTACHMENT A - SOIL SAMPLE SITE DESCRIPTIONS
Site No. Sample No. Site Descriptions
1. S29 Flat grassy area to north of facility buildings
2. S28 Front lawn area of Sheriff training center
3. S27 Covered lagoon area north of American Aggregate's access road and east
of ditch
4. S30 Flat grassy area to east of stacks on facility property
5. S3 3 Front yard area of Columbus Incinerator between the stacks and shredding
operations and east of the creek
6. S34 Front yard of facility slightly north of stacks
7. S25 Behind fenced in area around influent control site for Jackson Pike WWTP
east of Rt. 104
8. S24 North side of Jackson Pike WWTP and just north of the structure covering
Compost Filter 1.
9. S12 Entrance to Roadway Trucking Co property- high grassy knoll to the west
of the entrance drive south of Frank Rd. and east of 1-71
10. S13 West of office area for Agg Rok Materials off of Frank Rd. (711 Frank
Rd.)
11. S14 Scioto River levee approximately 1777 feet upstream of USGS gauging
station on Jackson Pike WWTP property
12. S15 Scioto River levee approximately 804 feet downstream of Jackson Pike
WWTP outfall structure.
13 S18 Scioto River Levee at extreme southeast corner of Jackson Pike WWTP
property (access from American Aggregates road)
14 SOS Flat area at top of landfill west of Jackson Pike and south of facility
15. S10 Private property south of Dyer Rd.-Tannis Dr.
A-l
-------
16. S11 Private property off Dyer Rd. at end of long tree covered lane
17. S09 Agg Rok Materials property off Brown Rd. opposite 2335 Brown Rd. flat
area above creek valley
18. S07 WMNI Radio tower site off Marlane Dr.
19 S26 Fill area at southwest corner of Jackson Pike WWTP
20. S22 Southwest corner of Berliner Park
21. S23 Berliner Park north of Jackson Pike grit chamber unit high flat grassy area
22. S19 American Aggregate's property off Haul Rd. site south of old quarry train
23. S20 Heritage Temple Baptist Church middle level of open grassy area
24. S21 Scioto Trail School open lawn area behind school
25. S06 Madison Plains School east of new high school high area of lawn to east of
package WWTP behind football practice field
26. S05 Madison Plains School east of new high school high grassy area even with
front of new high school
27. S04 Madison Plains School east of old high school
Quality control sample numbers: S01,S02,S03,S16,S17,S31,& S32
A-2
-------
ATTACHMENT B - LABORATORY ANALYSIS DATA SHEETS
-------
Key for Sample Analysis Data Sheets
Laboratory Identifying Number
47482-6-22
47482-6-16
47482-6-2
47482-6-3
47482-6-4
47482-6-5
47482-6-15
47482-6-6
47482-6-7
47482-6-20
47482-6-18
47482-6-19
47482-6-17
47482-6-8
47482-6-9
47482-6-10
47482-6-11
47482-6-12
47482-6-21
47482-6-23
47482-6-13
47482-6-14
47482-10-2
47482-10-3
47482-10-19
47482-10-20
47482-10-21
47482-10-22
47482-10-4
47482-10-5
47482-10-6
47482-10-7
47482-10-8
47482-10-9
47482-10-10
47482-10-11
47482-10-12
47482-10-13
47482-10-14
47482-10-15
47482-10-16
47482-10-17
47482-10-18
Description
Method Blank
SO I-Field Blank
S04 - Background Sample
S05 - Background Sample
S06 - Background Sample
S07
SI7-FieldBlank
SOS
S09
S09 - Laboratory Duplicate
S03 - Field Duplicate
S03 - Detection Limit Sample
S02 - Soil Reference Material
S10
Sll
S12
S13
SI4
S04 - Matrix Spike
S04 - Matrix Spike Duplicate
S15
S16-Field Duplicate
S18
S19
S34
S34 - Matrix Spike
S34 - Matrix Spike Duplicate
Method Blank
S20
S21
S22
S23
S24
S25
S26
S27
S28
S29
S30
S31 - Field Duplicate
S32-Field Blank
S33
S33 - Laboratory Duplicate
B-2
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 2-06-95
Ext. Date: 12-07-95
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
Lab Sample ID: 47482-6-22. METHOD
Sample Wt/Vol: 10.0000 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
Sample Data Filename: A037804
Blank Data Filename: A037803
Cal. Ver. Data Filename: A037802
ANALYTE
2.3.7.8-TCDD
l.2.3.7.8-PeCDD
1.2.3.4.7.8 HxCDD
1.2.3.6.7.8 HxCDD
1.2.3.7.8.9 II«CDD
1.2.3,4.6,7,8-HpCDD
OCDD
2.3,7.8-TCDF
1.2.3,7.8-PeCDF
2.3.4.7.8 PeCDF
l.2.3.4.7.8-HxCDF
1.2.3.6.7.8 HuCDF
l.2.3.7.8,9-HxCDF
2;3.4.6.7.8-HxCDF
Ti2?3.4.6.7.8-HpCDF
fa?3,4.7.8.9-HpCDF
OfcDF
Total Tem-Furans
Total Tetra-Dfoxins •
Total Pentt-Furans
Total Penta-Dioxinj
Total Hexa-Funns
Total Hexa-Dioxins
Total Hepta-Funns
Total Hepta-Dioxins
• Analyte not detected.
CONC.
FOUND
pg/g «IT
0.36
*
*
0.53
0.26
0.24
0.45
0.43
0.29
*
0.33
1.25
*
1.16
0.66
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION
pg'g dfy pg/g dfy
0.26
0.20
0.25
0.27
0.14
0.51
4.61
0.30
0.23
0.26
0.16
0.13
0.17
0.10
0.05
0.22
0.27
0.34
0.47
0.40
0.32
ION
RATIO
1.00
5.00
5.00
5.00
5.00
5.00
10.00
1.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
10.00
•
1.43
•
1.21
1.23
1.20
0.90
0.77
*
1.69
*
1.24
1.30
1.24
1.06
*
0.85
*
0.75
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
!3C-l.2.3.7.8-PeCDD
!3C-l.2.3.4.7.8-HxCDD
13C 1.2,3.6.7.8 HxCDD
13C 1.2,3.4.6.7.8 llpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-l,2.3.7,8-PeCDF
l3C-2.3,4.7.8-PeCDF
!3C-l.2,3.4.7.8-HxCDF
13C 1.2.3,6.7.8 HxCDF
13C 1.2.3,7.8.9 HxCDF
l3C-2.3.4,6.7.8-HxCDF
!3C-l.2.3.4.6.7.8HpCDF
13C 1.2,3.4.7,8.9 HpCDF
CLEANUP STANDARD
37CI 2.3,7.8-TCDD
SPIKE
CONC.
Pg
2000
2000
2000
2000
2(KX)
4000
2000
-2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1509
1428
1576
1728
1582
2641
1644
1699
1694
1642
1697
1555
1674
1612
1569
R(%)
75
71
79
86
79
66
82
85
85
82
85
78
84
81
78
ION
RATK
0.79
1.55
1.25
1.27
1 04
0.90
0.80
1.58
1.61
0.53
0.52
0.51
0.54
0.44
0.43
200
197
98
1.15
B-3
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-95
Ext. Date: 12-07-93
Analysis Date: I8-DEC-95 Time: 13:13:49
Extract Volume (uL): 20
Injection Volume (uL): I
ANALYTE
2.3,7.8-TCDD
J.2.3.7.8 PeCDD
1.2.3.4.7,8 HxCDD
J.2.3.6.7.8 HxCDD
1,2.3.7.8,9-HxCDD
j,2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8-TCDF
l.2.3.7.8-PeCDF
2.3.4.7.8 PeCDF
J.2.3,4.7.8-HxCDF
|.2.3.6.7.8-HxCDF
1.2.3.7.8.9 HxCDF
2,3.4,6.7,8 HxCDF
1.2.3,4.6.7.8 HpCDF
1.2,3.4.7.8.9 HpCDF
OCDF
Total Tetn-Furans
Total Tetn-Dioxiiu
Total Penta Furans
Total Penta-Dtoxins
Total Hexa-Furans
Total Hexa-Dioxini
Total Hepta-Funns
Total Hepta-Dbxins
CONC.
FOUND
pg/g dry
0.62
•
0.39
•
0.46
0.33
0.41
«
0.38
0.58
0.54
0.60
•
1.13
•
1.35
1.29
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO ION
pg/g dry pg/g dry RATIO
Lab Sample ID: 47482-6-16. SOI
Sample Wt/Vol: 10.1772 units:
Initial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A037806
Blank Data Filename: A037803
Cal. Ver. Data Filename: A037802
0.22
0.16
023
0.25
0.13
0.44
405
028
020
0.24
0.16
0.13
0.16
0.10
0.04
0.20
0.24
0.32
0.29
0.98
4.91
4.91
4.91
4.91
4.91
9.83
0.98
4.91
4.91
4.91
4.91
4.91
4.91
4.91
4.91
9.83
1. 10
0.87
0.86
•
1.65
1.17
0.91
•
0.96
0.68
0.70
1.48
•
1.27
•
0.91
1.13
!3C-l.2.3.7.8-PeCDD
l3C-l.2.3.4.7.8-HxCDD
13C-l.2.3.6.7.8-llxCDD
13C-1.2.3.4.6.7.8 HpCDD
I3COCDD
I3C-2.3.7.8-TCDF
!3C-l.2.3.7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
13C-1.2.3.4.7.8 HxCDF
I3C-1.2.3.6.7.8 HxCDF
I3C-1.2.3.7.8.9 HxCDF
l3C-2.3.4,6.7.8-HxCDF
I3C-I.2.3.4.6.7.8 HpCDF
l3C-l.2.3.4.7.8.9-llpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
P8
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CON
FOU
Pg
1593
1593
1582
1808
1666
2821
1549
1734
1654
1617
1579
1562
1609
1621
1590
R(%)
80
80
79
90
83
71
77
87
83
81
79
78
80
81
80
ION
RATIO
0.78
1.57
1.26
1.24
1.05
0.90
0.81
1 62
1.60
0.53
0.52
0.52
0.52
0.45
0.43
200
179
90
* Analyte concentration not quantified due to CDPE interference, see text for detail.
• Analyte not detected.
B-4
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-95
Ext. Date: 12-07-95
Analysis Date: I8-DEC-95 Time: 14:28:07
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
2,3.7.8-TCDD
.2.3.7.8-PeCDD
.2.3.4,7.8 HxCDD
.2,3.6.7.8 HxCDD
.2.3.7.8.9 HxCDD
.2,3,4.6.7.8-HpCDD
OCDD
2.3.7,8-TCDF
1.2,3,7.8-PeCDF
2,3.4.7.8-PeCDF
1,2.3.4,7.8 HxCDF
1.2,3.6,7.8-HxCDF
1.2.3.7.8.9 HxCDF
2,3.4,6.7.8 HxCDF
1.2.3.4.6.7.8 HpCDF
1.2.3.4.7.8.9 HpCDF
OCDF
Total Tetra
Total Tetra
Total Penta
Total Pent*
Total Hexa
Total Hexa
Total Hepta
Total Hepta
Furans
Dtoxins
•Furans
•Dioxins
Furans
Dioxins
Furans
Dioxins
CONC.
FOUND
Pg'gdry
*
•
0.74
1.39
2.11
31.60
298.32
0.55'
*
0.89
6.46
•
18.02
4.22
1.98
4.58
*
4.87
7.72
18.52
74.13
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRAT1O
pg/g dry pg/g dry
0.54
041
0.60
0.65
0.34
1.97
0.52
0.59
0.44
0.35
0.43
0.23
0.11
0.58
0.83
1.52
7.62
7.62
7.62
7.62
7.62
15.25
3.05
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
15.25
ION
RATIO
1.14
1.36
1.12
1.03
0.88
1.46
1.03
•
0.92
0.69
0.72
1.60
•
1.35
1.19
*
1.02
Lab Sample ID: 47482-6-2. S04
Sample Wl/Vol: 6.5575 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DBS
Sample Data Filename: A037807
Blank Data Filename: A037803
Cal. Ver. Data Filename: A037802
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
l3C-l.2,3.7.8-PeCDD
I3C-I.2.3.4.7.8 HxCDD
I3C-1.2.3.6.7.8 HxCDD
13C 1.2.3,4.6,7.8 HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-l,2,3.7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
13C-1.2.3.4,7.8 HxCDF
I3C 1.2,3.6.7,8-llxCDF
13C-1.2.3.7.8.9 HxCDF
l3C-2.3.4.6.7.8-HxCDF
l3C-l.2,3.4.6.7.8-HpCDF
13C-1.2.3,4,7.8.9 HpCDF
CLEANUPSTANDARD
37CI-2.3.7.8-TCDD
SPIKE
CONC.
P8
2000
2000
2000
2000
20(10
40tX)
2
-------
PCDO/PCDF ANALYSIS DATA SHEET
Ub Nime: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-93
Ext. Date: 12-07-95
Analysis Date: I8-DEC-95 Time: 15:34:43
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1.2,3.7.8-PeCDD
1.2,3.4.7.8 HiCDD
1.2.3.6.7.8 HxCDD
(,2,3.7.8.9-HxCDD
J.2.3.4.6.7.8-HpCDD
QCDD
2,3.7.8-TCDF
I.2.3.7.8-PeCDF
13.4,7.8-PeCDF
1.2,3.4.7,8-HxCDF
1.2.3.6.7.8 HxCDF
F 2.3.7.8.9 HxCDF
2.3.4.6.7.8 HxCDF
l.2.3.4.6.7.8-HpCDF
i.2.3.4.7,8.9 HpCDF
OCDF
Total Teira-Furans
Total Tetn-Dioxins
Total Penta-Funns
Total Penta-Dioxins
Total Hexa-Furans
Total Hexa-Dk>xins
Total Hepta-Furans
Total Hepu-Dioxins
CONC.
FOUND
Pg'g dry
0.34
*
»
O.S2
0.75
9.40
75.76
0.23'
0.55'
»
0.55
2.42
•
4.70
0.85
0.95
0.70
*
2.43
2.18
5.93
17.92
SAMPLE
LIMIT OF
DETECTION
pg/g dry
0.28
0.21
0.32
0.36
0.18
0.35
0.26
0.33
022
0 17
0.24
0.13
0.06
0.32
0.35
0.43
LOWEST
CALIBRATION
CONCENTRATIO
pg/g dry
1.25
6.26
6.26
6.26
6.26
6.26
12.52
1.25
6.26
6.26
6.26
6.26
6.26
6.26
6.26
6.26
12.52
ION
RATIO
0.69
*
*
1.46
1.37
1.09
0.86
0.65
1.20
1.08
•
0.89
0.81
0.88
1.45
*
1.18
1.17
Ub Sample ID: 47482-6-3. S05
Sample Wt/Vol: 7.9895 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DBS
Sample Data Filename: A037808
Blank Data Filename: A037803
Cal. Ver. Data Filename: A037802
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
!3C-l.2.3.7.8-PeCDD
13C-1.2.3.4.7.8 HxCDD
l3C-l,2.3.6.7.8-HxCDD
13C-1.2.3.4.6.7.8 HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-1.2.3.7,8-PeCDF
!3C-2.3.4.7,8-PeCDF
l3C-l.2.3,4.7.8-HxCDF
I3C-I.2.3.6.7.8 llxCDF
I3C-I.2.3.7.8.9 llxCDF
l3C-2.3.4.6.7.8-llxCDF
I3C-1.2.3.4.6.7.8 tlpCDF
13C-1,2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
C
F
P8
14
14
16
16
16
26
IS
IS
14
15
16
14
16
IS
13
R(X)
73
72
81
84
82
66
75
78
73
80
83
74
83
79
66
ION
RATIO
0.79
1.55
1.23
1.23
1.05
0.89
079
1.61
1.58
0.52
0.52
0.52
0.52
0.43
0.43
200
17 89
1.01
* Analyte concentration estimated; CDPE interference - see text for detail.
• Analyte not delected.
B-6
-------
PCDD/PCDF ANALYSIS DATA SHEET
Uh Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-95
Ext. Date: 12-07-95
Analysis Date: I8-DEC-95 Time: 16:41:51
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
CONC.
ANALYTE FOUND
P«'8 dry
2.3.7.8TCDD 0.57
1.2.3.7.8 PeCDD *
1.2,3.4.7.8 HxCDD •
1.2.3.6.7.8 HxCDD 0.54
1.2.3.7.8.9 HxCDD 0.83
1.2.3.4.6.7.8 HpCDD 12.20
OCDD 108.60
2.3.7.8-TCDF •
l.2.3.7.8-PeCDF *
2.3.4.7.8-PeCDF *
l.2.3.4.7.8-HxCDF *
1.2.3.6.7.8 HxCDF 0.47*
1.2.3.7.8.9 HxCDF *
2.3.4.6.7.8 HxCDF 0.47
l.2,3.4.6.7.8-HpCDF 3.30
1.2.3.4.7.8.9 HpCDF 0.35
OCDF 9.43
Total Tetra-Furans 1.70
Total Tetra-DioxinJ 0.99
Total Penta-Furans 1.05
total Penta-Dioxins *
Total Hexa-Furans 3.08
total Hexa-Dioxins 4.49
total Hepta-Furans 10.42
Total Hepta-Dioxins 21.26
Lab Sample ID: 47482-6-4. S06
Sample Wt/Vol: 8.2683 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A037809
Blank Data Filename: A037803
Cal. Ver Data Filename: A037802
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry pg/g dry RATIO
0.26
0.20
0.29
0.33
0.17
0.34
0.26
0.31
0.21
0.16
0.21
0.12
0.05
0.28
0.28
0.40
1.21
6.05
6.05
605
6.05
6.05
12.09
1.21
6.05
605
6.05
6.05
6.05
6.05
605
6.05
12.09
0.69
1.06
1.36
1.05
0.87
0.66
1.26
1.09
1.06
0.84
0.65
0.72
1.34
•
1.31
1.41
•
1.07
I3C-2.3.7.8-TCDD
l3C-l.2.3.7.8-PeCDD
l3C-l.2.3.4.7.8-HxCDD
13C 1.2.3.6.7.8 HxCDD
13C-1.2.3.4.6.7.8 HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
I3C 1.2.3.7.8 PeCDF
13C 2.3.4.7.8 PeCDF
l3C-l.2.3.4,7.8-HxCDF
l3C-l.2.3.6,7,8-HxCDF
I3C-I.2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3.4.6.7.8-HpCDF
l3C-l.2.3.4.7.8,9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
pg
2000
2000
2000
201)0
2(XK)
4000
2000
21100
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
PS
1367
1328
1517
1649
1569
2755
1318
1399
1338
I486
1506
1439
1585
1628
1289
ION
R(%) RATIO
68 0.77
66
76
82
78
69 (
66 I
70
67
.56
.28
.27
.03
)89
J.81
.61
.59
74 0.53
75 0.52
72 0.52
79 052
81 0.42
64 0.43
200
173
87
* Analyte concentration estimated; CDPE interference - see text for detail.
• Analyte not detected.
B-7
-------
PCDD/PCDF ANALYSIS DATA SHEET
Ub Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-93
Ext. Date: 124)7-95
Analysis Dale: I8-DEC-95 Time: 17:48:26
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
CONC.
ANALYTE FOUND
pg/g dry
2.3.7.8-TCDD •
1,2.3.7.8 PeCDD 1.12
1.2.3.4.7.8 HxCDD 1.05
1.2,3.6.7,8 HxCDD 1.20
1.2.3,7.8,9 HxCDD 1.47
r.2.3.4.6.7.8-HpCDD 11.69
0CDD 93.36
2.3.7.8-TCDFf 0.78
1.2.3.7,8-PeCDF 1.01
2,3.4,7.8-PeCDF 1.41
1.2,3,4.7.8 HxCDF 1.80'
1.2.3.6.7.8 HxCDF 1.70
j,2.3.7.8.9-HxCDF •
2.3.4.6.7.8 HxCDF 1.74
1.2.3.4.6.7.8 HpCDP 6.56
1.2.3.4.7.8.9 HpCDF •
OCDF 3.67
Total Tetra-Furans 7.56
Total Tetra-Dtoxins 4.04
Total Penta-Furans 12.61
Total Penta-Dioxins 3.61
Total Hexa-Furans 9.17
Total Hexa-Dioxins 9.24
Total Hepa-Furans 7.77
Total Hepta-Dioxins 22.96
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO ION
pg/g dry pg/g dry RATIO
0.4S
0.35
0.49
0.54
0.28
0.66
0.44
0.54
0.36
0.29
0.41
0.22
0.09
0.52
0.57
1.34
6.70
6.70
6.70
6.70
6.70
13.41
1.34
6.70
6.70
6.70
6.70
6.70
6.70
6.70
6.70
13.41
1.54
1.27
1.08
1.07
1.10
0.89
0.82
1.36
1.40
*
1.21
•
1.35
0.97
•
0.79
0.70
0.68
1.45
1.33
1.19
1.21
0.97
1.02
Lab Sample ID: 47482-6-5. S07
Sample Wt/Vol: 7.4596 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Auiospec
GC Column ID: 60M DBS
Sample Data Filename: A0378IO
Blank Data Filename: A037803
Cal. Ver. Data Filename: A037802
13C-2.3.7.8-TCDU
l3C-l.2.3.7.8PeCDD
l3C-l,2.3,4.7.8-HxCDD
I3C-I.2.3.6.7.8 HxCDD
I3C-I.2.3.4.6.7.8 HpCDD
13CCX:DD
I3C-2.3.7.8-TCDF
13C-1.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3.4.7.8-HxCDF
13C 1.2,3,6.7,8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
I3C-I.2.3.4.6.7.8 HpCDF
I3C-1.2.3.4.7.8.9 HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
P8
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
P8
1335
1201
1655
1748
1579
2537
1361
1290
1237
1576
1500
1379
1507
1622
1292
R(%)
,,:
60
83
87
79
63
68
64
62
79
75
69
75
81
65
ION
RATIO
0.76
1.56
1.24
1.25
1.05
0.89
0.79
1.57
1.58
052
0.50
0.52
051
0.43
0.42
200
156
78
12,3,7.8-TCDF value from second column confirmation.
" Analyte concentration estimated; CDPE interference - see text for detail.
* Analyte not detected.
B-8
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-93
Ext. Date: 12-07-95
Analysis Date: 19 DEC 95 Time. 11:00:03
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
2.3.7.8-TCDD
1.2,3.7.8 PeCDD
l.2.3.4.7.8-HxCDD
1.2.3.6.7.8 HxCDD
1,2.3,7.8,9 HxCDD
1,2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8-TCDF
1.2.3.7,8-PeCDF
2.3.4.7.8 PeCDF
1,2.3.4.7.8 H»CDF
1.2.3.6.7.8 HxCDF
l.2.3.7.8.9HiCDF
2.3.4.6.7.8-HxCDF
l.2.3.4.6.7.8-HpCDF
l,2,3.4,7,8.9HpCDF
OCDF
Total Ten-Furans
Total Tem-Dioxins
Total Penta-Furans
Total Penta-Dioxins
Total Hexa-Funns
Total Hexa-Dioxins
Total Hepta-Furans
Total Hepta-Dioxins
Lab Sample ID: 47482-6-15. SI7
Sample Wi/Vol: 10.0121 units:
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A037904
Blank Data Filename: A037903
Cal. Ver. Data Filename: A037902
CONC.
FOUND
pg/gdry
O.S8
*
0.26
0.38
0.32
0.34
4
0.60
SAMPLE
LIMIT OF
DETECTION
pg/g
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-95
Em. Date: 12-07-93
Analysis Date: 19 DEC 95 Time: 12:06:56
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
CONC.
ANALYTE FOUND
P8'8 dry
2.3.7.8 TCDD 1.52
1.2.3,7.8-PeCDD 1.41
1.2.3.4.7.8 HxCDD 1.12
1.2.3.6.7.8 HxCDD 1.46
,1.2.3.7.8.9 HxCDD 3.43
|,2.3.4.6.7.8-HpCDD 15.47
OCDD 312.42
2.3.7.8TCDFI 0.76
j,2.3.7.8-PeCDF 1.24
2.3.4.7.8 PeCDF 2.13
j.2.3.4.7.8-HxCDF 1.80'
1.2.3.6.7.8-HxCDF 1.71
j.2.3.7.8.9-HxCDF •
2.3.4,6.7,8 HxCDF 1.65
j,2.3.4,6.7.8 HpCDF 6.11
r.2.3.4.7.8.9-HpCDP 0.49
OCDF 2.36
Total Tetra-Funns 13.96
Total Tetra Dioxins 7.46
Total Penta Furans 15.61
Total Penta Dioxins 1.41
Total Hexa-Furans 9.37
Total Hexa-Dioxins 20.71
Total Hepta-Furans 6.60
Total Hepta Dioxins 38.11
SAMPLE . LOWEST
LIMIT OF CALIBRATION ION
DETECTION CONCENTRATIO RATIO
Pg/g dry Pg/g dry
0.39
0 16
0.20
0.23
0.34
0.31
0.36
0.42
0.32
0.13
0.25
0.11
0.35
1.20
6.00
6.00
6.00
6.00
6.00
11.99
1.20
6.00
6.00
6.00
6.00
6.00
6.00
6.00
6.00
11.99
0.82
1.59
1.19
1.12
1.07
0.98
0.86
0.84
1.67
1.49
*
1.20
•
1.25
1.14
1.01
0.82
0.85
0.84
1.55
1.59
1.09
1.23
•
1.07
Lab Sample ID: 47482-6-6. SOS
Sample Wt/Vol: 8.3373 units:
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A03790S
Blank Data Filename: A037903
Cal. Ver. Data Filename: A037902
g
I3C-2.3.7.8-TCDD
!3C-l.2.3.7.8-PeCDD
!3C-l.2.3.4,7.8-HxCDD
I3C-I.2.3.6.7.8 HxCDD
l3C-l.2.3.4.6.7.8-HpCDD
13C-OCDD
I3C-2.3.7.8-TCDF
I3C-I.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
I3C-I.2.3.4.7.8 HxCDF
I3C-1.2.3.6.7.8 HxCDF
l3C-l.2.3,7.8.9-HxCDF
l3C-2.3.4.6.7.8-HxCDF
l3C-l.2.3.4.6,7.8-HpCDF
I3C l.2.3.4.7,8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
P8
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
P8
1508
1554
1589
1742
1551
2856
1586
1585
1394
1595
1602
1592
1676
1511
1334
ION
R(%) RATIO
75 0.77
78
79
87
78
71 (
79 (
79
70
.56
.26
.25
.06
).89
).77
.60
.60
80 0.52
80 0.52
80 0.52
84 0.53
76 0.42
67 0.43
200
183 91
12.3,7,8-TCDF value from second column confirmation.
* Analyte concentration estimated: CDPE interference - see text for detail
• Analyte not detected.
B-10
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-06-95
Ext. Date: 12-07-95
Analysis Date: I9-DEC-95 Time: 13:14:56
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
? "
i.3.7.8-TCDD
i.2.3.7.8-PeCDD
l.2.3.4.7.8-HxCDD
1.2.3.6.7.8 HxCDD
1.2.3.7.8.9 HxCDD
1,2.3,4.6,7.8 HpCDD
OCDD
2,3.7.8-TCDF*
1.2,3.7,8-PeCDF
2.3.4.7,8-PeCDF
l.2.3.4.7.8-HxCDF
1.2,3.6.7.8 HxCDF
l.2.3.7.8.9-HxCDF
2.3,4.6.7.8-HxCDF
1,2.3.4.6.7.8 HpCDF
l.2.3.4.7.8.9-HpCDF
OCDF
Total Tetra-Furans
Total Tetra-Dioxins
Total Penta-Furans
Total Penta-Dioxins
Total Hexa-Furans
Total Hexa-Dioxins
total Hepta-Furans
Total Hepca-Dioxins
CONC.
FOUND
0.49
1.69
1.53
1.79
2.85
16.64
81.49
•
1.61
2.51
3.00*
2.57
•
2.62
11.54
0.73
6.76
21.67
11.70
21.46
7.85
15.29
22.15
17.56
31.68
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRAT1O
Pg'g dry Pg'g dry
0.36
061
0.20
0.26
0.28
3.21'
043
0.38
0.58
0.45
0.19
0.33
0.12
0.42
1.33
6.66
6.66
6.66
6.66
6.66
13.32
1.33
6.66
6.66
666
6.66
6.66
6.66
666
6.66
13.32
ION
RATIO
0.74
1.64
I.II
1.10
1.39
1.05
0.88
*
1.71
1.51
•
1.08
*
1.17
I.IS
0.90
0.89
0.78
0.79
1.50
1.43
1.18
1.17
•
1.07
Lab Sample ID: 47482-6-7. S09
Sample Wt/Vol: 7.5058 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Auiospec
GC Column ID: 60M DBS
Sample Data Filename: A037906
Blank Data Filename: A037903
Cal. Ver. Data Filename: A037902
SPIKE CONC. ION
LABELED COMPOUNDS CONC. FOUN R(%) RATIO
Pg Pg
I3C-2.3.7.8-TCDD
!3C-l.2.3.7.8-PeCDD
!3C-l.2.3.4.7.8-llxCDD
I3C-I.2.3.6.7.8-IUCDD
1 3C- 1 ,2.3,4.6.7,8-HpCDD
I3C-OCDD
13C-2.3.7.8-TCDF
1 3C-1. 2.3.7.8 PeCDF
!3C-2,3.4.7.8-PeCDF
l3C-l.2.3.4.7.8-HxCDF
l3C-l.2.3.6.7,8-llxCDF
13C-I.2.3.7.8.9 HxCDF
I3C 2.3.4.6.7.8 HxCDF
I3C-I.2.3.4.6.7.8 HpCDF
I3C- 1.2.3.4.7.8.9 HpCDF
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000 •
2000
2000
2000
2000
2000
1166
1133
1425
1458
1398
2506
1206
1249
1273
1255
1225
1181
1361
1429
1220
58
57
71
73
70
63
60
62
64
63
61
59
68
71
61
0.77
1.50
1.26
1.27
1 03
0.90
0.78
1 59
1 59
0.52
0.51
052
0.53
045
0.44
CLEANUP STANDARD
37CI-2.3.7.8 TCDD
200
147
73
* 2,3,7.8-TCDF value from second column confirmation.
* Sample limit of detection (LOD) higher than lowest calibration concentration.
" Analyte concentration estimated; CDPE interference - see text for detail.
• Analyte not detected.
B-ll
-------
PCDD/PCDF ANALYSIS DATA SHEET
Ub Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-06-95
Ext. Dale: 12-07-95
Analysis Date: I9-DEC-95 Time: 14:23:23
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
CONC.
ANALYTE FOUND
Pg/g dry
2.3.7.8TCDD 0.54
1,2.3.7.8 PeCDD 2.41
1.2.3.4.7.8 HxCDD 2.00
1.2.3.6.7,8 HxCDD 2.33
1.2.3.7.8.9 HxCDD 4.16
l.2.3,4.6.7.8-HpCDD 19.71
OCDD 89.99
2.3.7.8-TCDF* 2.03
j.2.3.7.8 PeCDF 1.73
2.3.4.7.8 PeCDF 3.70
1.2.3.4.7.8 HxCDF 1.50'
J.2.3.6.7.8-HxCDF 3.89
1,2,3.7.8.9-HxCDF 0.36
2.3.4.6.7.8 HxCDF 3.36
T.2.3.4.6.7.8-HpCDF 13.82
jk2.3.4.7.8.9-HpCDF 1.04
(SCDF 7.87
Total Tetra-Furans 27.12
Total TetnDioxins 11.34
Total Penta-Furant 35.16
Total Penta-Dioxins 3.57
Total Hexa-Furans 19.55
Total Hexa-Dioxins 28.40
Total Hepta-Furans 21.69
Total Hepta-DioxinJ 36.35
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO
pg/g dry pg/g dry
0.26
046
0.17
022
024
0.33
0.31
0.45
0.34
0.13
0.26
0.10
0.37
1.33
6.65
6.65
6.65
6.65
6.65
13.30
1.33
6.65
6.65
6.65
6.65
6.65
6.65
6.65
6.65
13.30
ION
RATIO
0.75
.72
.33
.35
.34
.02
0.86
0.83
.59
.50
*
.25
.11
.15
.08
0.99
0.92
0.73
0.75
1.48
1.67
1.36
1.22
•
1.06
Lab Sample ID: 47482-6-20. S09. Duplicate
Sample Wt/Vol: 7.5170 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A037907
Blank Data Filename: A037903
Cal. Ver. Data Filename: A037902
LABELED COMPOUNDS
I3C-2.3.7.8TCDD
l3C-l.2,3.7.8-PeCDD
!3C-l.2.3.4.7.8-HxCDD
l3C-1.2.3.6.7.8-HxCDD
1 3C- 1 ,2.3.4,6,7.8-HpCDD
I3COCDD
I3C-2.3.7.8 TCDF
I3C-I.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3.4.7.8-HxCDF
I3C- 1.2.3,6.7.8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
l3C-2.3.4.6.7.8-HxCDF
1 3C- 1 .2.3.4 ,6.7.8-HpCDF
l3C-1.2.3.4.7.8.9-HpCDF
SPIKE
CONC
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUN
Pg
1356
1227
1554
1570
1588
2724
1318
1335
1281
1479
1459
1568
1560
1461
1350
68
61
78
78
79
68
66
67
64
74
73
78
78
73
68
ION
RATIO
0.78
1.53
1.26
1.26
1.02
0.88
0.77
1.60
1 61
0.51
0.50
0.51
0.52
0.43
0.43
CLEANUP STANDARD
37CI-2.3.7.8 TCDD
200
169
84
12.3.7,8-TCDF value from second column confirmation.
' Analyte concentration estimated; CDPE interference - see text for detail.
* Analyto not delected.
B-12
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-95
Ext. Date: 12-07-95
Analysis Date: I9-DEC-95 Time: 16:36:31
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: 1:2
ANALYTE
2.3.7.8TCDD
1.2.3.7.8 PeCDD
1.2.3.4.7.8 HxCDD
1.2.3,6.7,8-HxCDD
1.2.3,7.8.9 HxCDD
1.2.3.4,6.7.8 HpCDD
OCDD
2.3.7.8-TCDF*
l.2.3.7.8-PeCDF
2.3,4.7.8 PeCDF
l.2.3.4.7,8-HxCDF
l.2.3.6.7.8-HxCDF
1.2.3.7.8.9-HxCDF
2.3.4.6.7,8-HxCDF
1.2.3.4.6.7.8 HpCDF
l.2.3,4.7.8.9-HpCDF
OCDF
Total Telra-Furans
Total Tetra-Dioxins
Total Penta-Furans
Total Penta-DJoxins
Total Hexa-Furans
Total Hexi-Dtoxim
Total Ilepa-Punni
Total Hepta-Dk>xins
CONC.
FOUND
Pg'g dry
»
*
1.48
1.67
2.00
28.00
285.65
1.60
1.97
2.10
0.84
2.00
7.40
1.38
18.28
2.06
*
6.23
20.63
64.01
Lab Sample ID: 47482-6-18. S03
Sample Wt/Vol: 6.6061 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A037909
Blank Data Filename: A037903
Cal. Ver. Data Filename: A037902
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION
pg/8
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-06-95
Ext. Date: 12-07-95
Analysis Dale: I9-DEC-95 Time: 17:32:10
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: 1:2
CONC.
ANALYTE FOUND
P8/g dry
2.3.7.8TCDD 9.64
1.2,3.7.8 PeCDD 46.40
1.2.3.4.7,8 HxCDD 40.54
1,2.3.6.7.8 HxCDD 35.90
1.2.3.7.8.9 HxCDD 39.03
1,2,3,4.6.7.8 HpCDD 60.44
QCDD 270.77
2.3.7.8-TCDF 9.82
i.2.3.7.8-PeCDF 40.52
2.3,4.7.8 PeCDF 43.62
j.2.3.4.7.8-HxCDF 40.79
j.2.3.6.7,8 HxCDF 42.32
1-.2.3.7.8.9 HxCDF 42.32
2.3.4.6.7.8 HxCDF 40.64
l2.3.4.6.7.8-HpCDF 38.85
ii2.3.4.7.8.9-HpCDF 40.83
OCDF 87.91
v*
Total Tetra-Furans 9.82
Total Tetra-Dioxins 9.64
Total Pema-Furans 86.18
Total Penta-Dioxins 46.40
Total Hexa Furans 169.51
Total Hexa Dioxins 115.47
Total Hepta-Furans 79.68
Total Hepta-Dioxins 89.91
SAMPLE
LIMIT OF
DETECTION
pg/g dry
LOWEST
CALIBRATION ION
CONCENTRATIO RATIO
pg/g dry
6.05 0.71
30.24
30.24
30.24
30.24
30.24
60.48 (
6.05 (
30.24
30.24
30.24
30.24
30.24
30.24
30.24
30.24
.43
.30
.28
.14
.01
).90
).77
.54
.52
.17
.19
.30
.22
.01
.05
60.48 0.85
*
0.71
1.74
1.43
1.26
1.30
*
1.06
Lab Sample ID: 47482-6-19. S03. DL Spike
Sample Wt/Vol: 6.6138 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DBS
Sample Data Filename: A0379IO
Blank Data Filename: A037903
Cal. Ver. Data Filename: A037902
I3C-2.3.7.8-TCDD
l3C-l.2.3,7.8-PeCDD
!3C-l.2.3.4.7.8-HxCDD
I3C-I.2.3.6.7.8-HXCDD
I3C-I.2.3.4.6.7.8 HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-l.2.3.7.8-PeCDF
!3C-2.3.4,7.8-PeCDF
l3C-l.2.3.4.7,8-HxCDF
I3C-1.2.3.6.7.8 HxCDF
I3C-1.2,3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3,4.6.7.8HpCDF
I3C l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
P8
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
Pg
1386
1351
1545
1664
1623
3012
1409
1366
1346
1438
1397
1536
1537
1492
1371
ION
R(») RATIO
69 0.78
68
77
83
81
75 <
70 1
68
67
.60
.25
.24
.03
)89
).82
.58
.59
72 053
70 O.SI
77 051
77 0.52
75 0.42
69 0.43
200
164
82
B-14
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-93
Ext. Date: 12-07-93
Analysis Date: I9-DEC-95 Time: 18:38:11
Extract Volume (uL): 20
Injection Volume (uL): 1.0
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1.2.3.7,8-PeCDD
(.2.3.4.7.8 HuCDD
1.2.3.6.7.8 HxCDD
1,2,3.7.8.9-HxCDD
l.2,3.4.6.7.8-HpCDD
OCDD
2.3.7.8-TCDF
1.2.3.7,8-PeCDF
2.3,4.7,8-PeCDF
l.2.3.4,7.8-HxCDF
1.2.3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2.3.4.6.7.8 HxCDF
1.2.3.4.6.7,8 HpCDF
1.2.3.4.7.8.9 HpCDF
OCDF
Total Tetra
Total Tetra-
Total Perm
Total Penta
Total Hexa
Total Hexa
Total Hepta
Total Hepta
Furans
•Dioxins
•Furans
•Dioxins
Furans
Dioxins
i-Furans
i-Dioxins
CONC.
FOUND
pg/g dry
486.79
1072.82
941.48
864.43
926.91
1430.33
3086.77
467.75
923.28
972.43
965.78
942.33
1010.55
936.04
1332.23
1414.48
2348.15
467.75
486.79
1897.71
1072.82
3854.70
2732.84
2746.71
1464.93
SAMPLE LOWEST
LIMIT OF CALIBRATION ION
DETECTION CONCENTRATIO RATIO
pg/g dry pg/g dry
1.00
5.00
5.00
5.00
5.00
5.00
10.00
1.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
10.00
0.77
1.54
1.24
1.24
1.24
1.06
0.88
0.76
1.53
1.52
1.21
1.21
1.22
1.20
1.00
1.00
0.86
0.77
1.33
1.54
1.21
1.24
1.00
1.06
Lab Sample ID: 47482-6-17. S02.
Sample Wt/Vol: 10.0000 units:
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A0379II
Blank Daia Filename: A037903
Cal. Vcr. Data Filename: A037902
g
LABELED COMPOUNDS
13C 2.3.7.8 TCDD
!3C-1.2.3.7.8-PeCDD
I3C-1 ,2.3,4.7,8-HxCDD
I3C-I.2.3.6.7.8 HxCDD
1 3C- 1 ,2.3.4.6,7,8-HpCDD
I3COCDD
I3C-2.3.7.8-TCDF
l3C-l,2.3.7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2,3.4.7,8-HxCDF
I3C 1.2,3.6.7.8 HxCDF
l3C-l.2.3.7.8.9-HxCDF
l3C-2.3.4.6.7.8-HxCDF
l3C-1.2.3,4.6.7.8-HpCDF
I3C-I.2.3.4.7.8.9 HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2(NK)
2000
2000
2000
2000
2000
CONC
FOUN
P8
1436
1420
1480
1503
1592
2865
1381
1464
1385
1374
1382
1536
1396
1427
1496
R(%)
72
71
74
75
80
72
69
73
69
69
69
77
70
71
75
ION
RATIO
0.78
1.56
1.22
1.24
1.04
0.89
0.79
1.58
1.60
0.52
0.52
0.51
0.51
0.44
0.43
CLEANUP STANDARD
37CI-2.3.7.8 TCDD
200
175
87
B-15
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-95
Ext. Date: 12-07-93
Analysis Date: l5-JAN-96Time: 11:10:41
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
Lab Sample ID: 47482-6-8. S10
Sample Wt/Vol: 6.8140 units: g
Initial Calibration Dale: 04-13-93
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A0389O4
Blank Data Filename: A038903
Cal. Ver. Data Filename: A038902
ANALYTE
2.3,7.8-TCDD
,2.3.7.8-PeCbD
,2.3.4.7.8 HxCDD
.2.3.6.7.8 HxCDD
.2.3.7.8.9-HxCDD
.2.3.4.6.7,8-HpCDD
OCDD
2.3.7.8-TCDF
1.2.3.7.8 PeCDF
2.3.4.7.8 PeCDF
j.2.3.4.7.8 HiCDF
J.2.3.6,7.8-HxCDF
i;2.3.7.8.9-HxCDF
2.3.4.6.7.8 HxCDF
1.2.3.4.6.7.8 HpCDF
i:i.3.4.7.8.9-llpCDF
OCDF
Tout Tetra-Furans
Toul Tetra-Dioxins
Total Pentt-Furans
Toul PenU-Dbxins
Tool Hexa-Furans
Toul Hexa-Dioxins
Toul Heptt Furans
Toul Hepu-Dioxirts
CONC.
FOUND
pg/gdry
0.74
2.42
3.76
369
8.83
143.09
1204.99
(4.00)
1.93
4.55
6.50'
3.39
*
3.43
37.32
2.51
81.41
78.74
8.25
30.94
2.42
43.33
35.54
104.54
256.53
SAMPLE
LIMIT OF
DETECTION
pg/gdry
0.15
0.29
0.35
0.21
0.25
0.21
0.21
0.32
0.13
0.09
0.78
LOWEST
CALIBRATION
CONCENTRATIO
pg/g dry
1.47
7.34
7.34
7.34
7.34
7.34
14.68
1.47
7.34
7.34
7.34
7.34
7.34
7.34
7.34
7.34
14.68
ION
RATIO
0.69
1.58
1.28
1.32
1.22
1.08
0.88
(0.74)
1.58
1.39
*
I.I!
•
1.21
1.05
1.03
0.87
0.79
0.67
1.62
1.58
1.28
1.31
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
l3C-l.2.3.7.8-PeCDD
l3C-l.2.3.4.7.8-HxCDD
l3C-l,2.3.6.7.8-HxCDD
I3C-1. 2.3.4 ,6.7,8-HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
I3C-1. 2.3.7,8 PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3.4.7.8-HxCDF
I3C-1. 2.3,6.7.8 HxCDF
l3C-l.2.3.7.8.9-HxCDF
I3C-2.3.4.6.7.8 HxCDF
I3C-1 .2.3.4.6.7.8-HpCDF
I3C-I.2.3.4.7.8.9IIPCDF
SPIKE
CONC.
Pg
2000
2000
2(NN)
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
Pg
1493
1590
1499
1658
1530
2738
1484
1594
1582
1533
1563
1565
1629
1645
1481
75
79
75
83
77
68
74
80
79
77
78
78
81
82
74
ION
RATIO
0.78
1.57
1 24
| 25
1 02
0.88
0.77
1.57
1.57
0 51
0 51
0 31
0.52
0 43
0.43
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
192
96
1.04
() Second column confirmation not done. 2.3.7.8-TCDF concentration estimated: see text for deuil.
'Analyte concentration estimated: CDPE interference • see text for detail.
* Analyte not delected.
B-16
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-06-95
Ext. Dale: 124)7-95
Analysis Date: 15-JAN 96Time: 12:39:50
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
V - .,
2.3.7.8TCDD
1.2.3.7,8-PeCDD
1,2,3.4,7.8-HxCDD
1,2,3.6.7.8 HxCDD
1.2.3.7,8,9-HxCDD
l.2.3.4.6.7,8-HpCDD
OCDD
2.3.7.8-TCDF
1.2.3.7,8-PeCDF
2.3.4.7,8-PeCDF
l.2.3.4.7.8-HxCDF
1.2.3.6.7.8 HxCDF
1.2.3,7.8.9 HxCDF
2.3,4,6.7.8-HxCDF
l.2.3.4.6.7.8-HpCDF
l.2.3.4.7.8,9-HpCDF
OCDF
Total Tetn-Furans
Total Tetra-DJoxins
Total Penta-Furans
Total Penta-DJoxins
Total Hexa-Furans
Total Hexa-Dioxins
Total Hepu-Furans
Total Hepca-Dioxins
CONC.
FOUND
pg/gdry
0.79
2.84
2.95
3.37
6.71
31.22
124.76
(2.11)
2.15
3.88
4.30'
4.00
•
4.49
23.83
1.59
32.95
37.50
10.80
45.76
22.37
23.95
40.95
36.08
57.44
Lab Sample ID: 47482-6-9. SI I
Sample Wt/Vol: 7.5250 unils: g
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DBS
Sample Data Filename: A038905
Blank Data Filename: A038903
Cat. Ver. Data Filename: A038902
SAMPLE LOWEST
LIMIT OF CALIBRATION ION
DETECTION CONCENTRATIO RATIO
Pg'g dry Pg/g dry
0.12
0.23
0.26
0.16
0.19
0.17
0.17
0.25
0.10
0.07
0.58
1 33
6.64
6.64
6.64
6.64
6.64
13.29
1.33
6.64
6.64
6.64
6.64
6.64
6.64
6.64
6.64
13.29
0.71
1.55
1.32
1.24
1.25
1.04
0.88
(0.79)
1.34
1.45
*
1.13
- •
1.16
1.00
0.93
0.89
0.68
0.74
1.56
1.53
1.22
1.37
I3C 2.3,7,8-TCDD
!3C-1.2.3.7.8-PeCDD
I3C-I.2.3.4.7.8 HxCDD
l3C-l,2.3.6,7,8-HxCDD
l3C-l,2.3,4,6.7.8-HpCDD
I3COCDD
13C-2.3.7.8-TCDF
l3C-l,2.3,7,8-PeCDF
!3C-2,3.4.7,8-PeCDF
I3C-I.2.3.4.7.8 HxCDF
13C-I.2.3.6.7.8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3,4,6.7.8-llpCDF
13C 1.2,3.4.7.8.9 HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC
pg
2000
2000
2000
201)0
2000
4000
2000
2IXX)
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
P8
1547
1608
1555
1684
1550
2894
1482
1680
1604
1557
1530
1581
1656
1551
1462
ION
R(%) RATIO
77 0.80
80
78
84
77
72 (
74 (
84
80
.55
.34
.17
.05
).89
)8I
.57
.60
78 0.52
76 053
79 0.51
83 0.52
78 0.44
73 0.44
200
205
102
1.08
( ) Second column confirmation not done. 2.3.7.8-TCDF concentration estimated; see text for detail.
' Analyle concentration estimated: CDPE interference, see text for detail.
* Analyte not delected. ;
B-17
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-06-95
Ext. Date: 12-07-95
Analysis Date: 15 JAN-96Time: 13:48:39
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1.2.3,7.8-PeCDD
1.2.3.4.7.8 HxCDD
1,2.3.6.7.8 HxCDD
1.2.3.7.8.9 HxCDD
1.2,3.4.6.7,8 HpCDD
OCDD
2.3.7.8TCDF
1,2.3.7.8-PeCDF
2.3.4,7,8 PeCDF
j.2.3.4.7.8 HxCDF
i,.2.3.6.7,8-HxCDF
l.2.3.7.8.9-HxCDF
2.3.4.6.7.8 HxCDF
l.2.3.4.6.7.8-HpCDF
i<2.3.4.7,8.9 HpCDF
OCDF
Total Tetra-Furans
Total Tetra Dioxins
Total Pema-Furans
Total Pema-Dioxins
Total Hexa-Furans
Total Hexa-Dtoxins
Total Hepu-Furans
Total Hepta-Dloxins
CONC.
FOUND
Pg'g dry
0.54
2.06
2.20
2.49
2.75
24.99
142.08
(1.26)
2.24
2.88
3.20'
3.33
0.17
3.33
14.29
1.04
13.10
17.02
3.60
30.25
7.82
21.30
18.87
22.99
46.84
SAMPLE LOWEST
LIMIT OF CALIBRATION ION
DETECTION CONCENTRATIO RATIO
pg/g dry pg/g dry
020
0.41
0.42
0.25
0.34
0.33
0.27
0.28
0.42
0.16
0.12
1.00
1.31
6.53
6.53
6.53
6.53
6.53
13.06
1.31
6.53
6.53
6.53
6.53
6.53
6.53
6.53
6.53
13.06
0.85
1.69
1.38
1.30
1.29
1.05
0.87
(0.75)
1.35
1.33
•
1.14
•
1.37
1.01
1.17
0.84
0.68
0.76
1.63
1.73
1.05
1.23
Lab Sample ID: 47482 6-10. SI2
Sample Wt/Vol: 7.6567 units:
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A038906
Blank Data Filename: A038903
Cal. Ver. Dais Filename: A038902
g
I3C2.3.7.8-TCDD
l3C-l.2.3,7,8-PeCDD
l3C-1.2.3,4.7,8-HxCDD
!3C-l.2.3.6,7.8-HxCDD
I3C 1.2.3.4.6.7.8 HpCDD
13C-OCDD
13C 2.3.7.8 TCDF
)3C-l,2,3.7,8-PeCDF
l3C-2,3.4,7.8-PeCDF
!3C-l.2.3.4.7.8-HxCDF
13C-1.2.3.6.7.8 HxCDF
I3C-1.2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3.4.6.7.8-HpCDF
I3C l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC
pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
20(10
2000
2000
2000
2000
CONC.
FOUND
Pg
1391
1337
1468
1555
1498
2300
1387
1397
1361
1386
1382
1422
1429
1452
1336
R(%)
70
67
73
78
75
58
69
70
68
69
69
71
71
73
67
ION
RATIO
0.78
1.53
1.23
1.25
1.03
0.88
0.78
1.55
1.56
0.52
052
052
O.SI
0.45
0.43
200
154
77
1.01
() Second column confirmation not done.
• Analyte not detected.
"Analyte concentration estimated: CDPE
interference; see text for detail.
2.3.7.8-TCDF concentration estimated; see text for detail.
B-18
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-07-95
Ext. Date: 12-07-95
Analysis Dale: I5-MN-96 Time: 14:57:09
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
5.3.7.8-TCDD
'1.2.3.7.8 PeCDD
1,2,3.4.7.8 HuCDD
j,2.3.6.7,8llxCDD
'},2,3.7.8.9 HxCDD
0.3,4,6.7.8-HpCDD
OCDD
2.3.7.8-TCDF
1.2,3.7.8 PeCDF
2.3.4.7,8 PeCDF
1.2.3.4.7.8 HxCDF
1.2,3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2.3.4.6.7.8 HxCDF
l.2.3.4.6.7.8-HpCDF
1.2,3.4,7.8.9 HpCDF
OCDF
Tout Ten
Total Ten
Total Pent*
Total Penu
Total Hexa-
Total Hexa
Total Hepta
Total Hepu
Furans
Dioxins
•Funns
•Dioxins
Furans
Dioxins
Furans
-Dioxins
CONC.
FOUND
pg/g dry
0.67
3.41
3.23
3.81
5.21
29.20
126.12
(2.15)
2.73
4.92
4.90'
4.91
0.25
4.80
20.96
1.59
11.18
40.17
15.71
50.32
20.64
24.82
44.22
32.65
55.01
Lab Sample ID: 47482-6-11. SI3
Sample Wt/Vol: 8.0366 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A038907
Blank Data Filename: A038903
Cal. Ver. Data Filename: A038902
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO
pg/g dry pg/g dry
0.14
0.28
0.34
0.20
0.27
0.23
0.21
0.23
0.33
0.12
0.09
0.77
0.55
ION
RATIO
1.
6.
6.
6.
6.
6.
12
1.
6.
6.
6.
6.
6.
6.
6
6.
12
24 (
22
22
22
22
22
44 (
24 ((
22
22
22
22
22
22
22 (
22 (
.44 (
(
(
).67
.53
.31
.18
.22
.05
).89
).72)
.62
.60
•
.25
•
1.15
).99
).94
).87
).79
).68
.48
.48
1.28
1.25
*
1.05
LABELED COMPOUNDS
I3C-2.3.7.8 TCDD
I3C-1. 2.3.7.8 PeCDD
I3C-I.2.3.4.7.8-HXCDD
l3C-l.2.3.6.7.8-llxCDD
I3C-1.2 3 4 6.7,8-HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
I3C 1,2.3.7.8-PeCDF
I3C 2.3.4.7.8 PeCDF
I3C-I 2 3.4.7 8-llxCDF
l3C-l,2.3.6.7.8-llxCDF
l3C-1.2.3.7.8,9-HxCDF
l3C-2.3.4.6.7.8-HxCDF
1 3C- 1 ,2.3.4 ,6.7.8-HpCDF
I3C 1,2.3.4 ,7 .8,9 HpCDF
SPIKE
CONC
P8
20(10
20110
2(XK)
2 (XX)
2000
4000
2000
2000
2000
20110
20110
2000
2000
2000
2000
CONC.
FOUND
Pg
1436
1326
1386
1554
1524
2679
1311
1392
1348
1380
1403
1537
1473
1482
1407
ION
R(%) RATIO
72 0.78
66 1
69 1
78 1
76 1
67 (
66 I
70 1
67 1
1.52
1.26
1.29
1.04
).89
).8I
1.59
1.59
69 0.52
70 0.52
77 0.51
74 0.52
74 0.44
70 0.43
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
160
80
( ) Second column confirmation not done. 2.3.7.8-TCDF concentration estimated; see text for detail.
' Analyte concentration estimated; CDPE interference, see text for detail
• Analyte not detected.
B-19
-------
PCDD/PCDF ANALYSIS DATA SHEET
Ub Name: BATTELLE
Matrix: SOIL
Sample Receipi Date: 12-07-93
Exl. Date: 1247-93
Analysis Date: I3-JAN-96 Time: 16:06:00
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
CONC.
ANALYTE FOUND
pg/gdry
2.3.7.8-TCDD 10.91
1.2,3.7.8-PeCDD 4.08
1.2.3.4,7,8 HxCDD 3.90
1.2.3.6.7.8 HxCDD 7.34
1.2.3.7.8,9 HxCDD 5.93
1.2,3.4.6.7.8 HpCDD 127.53
OCDD 997.01
2.3.7.8-TCDF (3.92)
1.2.3.7,8-PeCDF 4.14
2.3.4.7.8-PeCDF 5.79
1,2.3.4.7.8 HxCDF 5.70-
1.2.3.6.7.8 HxCDF 5.04
1.2.3.7.8.9 HxCDF •
2,3,4.6.7.8 HxCDF 4.76
}.2,3.4,6.7.8 HpCDF 30.87
j.2.3.4.7.8,9-HpCDF 1.70
OCDF 31.49
Total Tetra-Furans 86.66
Total Tetra-Dioxins 32 1?
.Total Penta-Furans 63 .'ft
total Penta Dkuins 4.08
Total Hexa Furans 42.85
Total Hexa Dioxins 62.86
Total Hepta Furans 64.79
Total Hepta-Dioxins ' 230.85
SAMPLE
LIMIT OF
DETECTION
pg'gdry
0.29
0.32
0.26
0.25
0.21
0.23
0.34
0.13
0.10
0.83
LOWEST
CALIBRATION
CONCENTRATIO
pg/g dry
1.37
6.85
6.85
6.85
6.85
6.85
13.71
1.37
6.85
6.85
6.85
6.85
6.85
6.85
6.85
6.85
13.71
ION
RATIO
0.73
.67
.11
.24
.15
.06
0.87
(0.81)
.42
.45
*
1.22
*
1.23
0.97
1.02
0.86
0.69
0.76
1.53
1.67
1.12
1.19
*
1.04
Lab Sample ID: 47482-6-12. SI4
Sample Wt/Vol: 7.2963 units:
Iniiial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A038908
Blank Data Filename: A038903
Cal. Ver. Data Filename: A038902
8
LABELED COMPOUNDS
I3C-2.3.7.8TCDD
!3C-l.2.3.7.8-PeCDD
I3C-I.2.3.4.7.8 HxCDD
!3C-1.2.3.6.7.8-HxCDD
l3C-l.2,3,4.6.7.8-HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
I3C- 1.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3,4.7.8-HxCDF
l3C-l,2.3,6.7.8-llxCDF
I3C-1. 2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8-HXCDF
l3C-l,2.3.4.6.7.8-HpCDF
13C-1.2.3.4.7.8.9-HpCDF
SPIKE
CONC
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2(X»
2INX)
2000
2000
2000
2000
CONC.
FOUN
Pg
1247
1234
1325
1463
1286
2370
1170
1239
1198
1244
1187
1290
1291
1251
1129
R(%)
62
62
66
73
64
59
58
62
60
62
59
65
65
63
56
ION
RATIO
0.80
1.54
1.22
1.26
1.04
0.89
0.81
1.58
1.57
0.52
0.51
0.51
0.52
0.44
0.42
CLEANUP STANDARD
37CI-2.3.7.8-TCDD 200
141
70
() Second column confirmation not done. 2.3.7.8-TCDF concentration estimated; see text for detail.
" Analyte concentration estimated: CDPE interference, see text for detail.
• Analyte not detected.
B-20
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-06 95
Ext. Date: 12-07-95
Analysis Date: 15-JAN-96 Time: 17:12:38
Extract Volume (uL): 20
Injection Volume (uL): I
'Dilution Factor: NONE
ANALYTE
,2.3.7,8TCDD
;i.2.3.7.8-PeCDD
|l. 2.3.4,7.8 HxCDD
,1.2.3.6.7,8 HxCDD
tl. 2.3.7.8.9 HxCDD
1.2.3.4.6.7.8 HpCDD
2.3.7.8-TCDF
1.2.3,7.8-PeCDF
2.3.4.7.8-PeCDF
1. 2.3.4.7.8 HxCDF
1.2,3.6.7.8 HxCDF
1. 2.3.7.8.9 HxCDF
2.3.4.6,7.8-HxCDF
1.2,3.4.6.7.8 HpCDF
l.2.3.4.7.8,9-HpCDF
OCDF
Total Tcira
Total Tetra
Total Penta-
Total Penla
Total Hexa
Total Hexa-
Total llepta
Total Hepta
•Furans
•Dioxins
•Furans
•Dioxins
'Furans
•Dioxins
•Furans
i-Dioxins
CONC.
FOUND
Pg/gdry
37.23
193.83
168.85
147.66
160.72
191.35
544.99
35.49
167.14
169.57
172.18
172.44
179.73
169.94
158.59
171.61
359.45
36.31
37.23
336.70
193.83
694.29
477.23
340.29
218.67
SAMPLE
LIMIT OF
DETECTION
Pg/gdry
LOWEST
CALIBRATION ION
CONCENTRATION RATIO
pg/g dry
1.52 0.76
7.62
7.62
7.62
7.62
7.62
15.25 (
1.52 (
7.62
7.62
7.62
7.62
7.62
7.62
7.62
7.62
.56
.34
.21
.23
.08
).88
).77
.55
.54
.25
.18
.24
.21
.00
.00
15.25 0.91
0.87
0.76
1.55
1.56
*
1.34
1.05
Lab Sample ID: 47482-6-21. S04, MS
Sample Wi/Vol: 6.5583 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A038909
Blank Data Filename: A038903
Cal. Ver. Data Filename: A038902
SPIKE
LABELED COMPOUNDS CONC
Pg
I3C-2, 3.7.8 TCDD
!3C-l.2.3.7.8-PeCDD
!3C-1.2.3.4.7.8-HxCDD
l3C-l.2.3.6.7.8-llxCDD
l3C-l.2.3.4,6.7.8-HpCDD
13COCDD
I3C-2.3.7.8-TCDF
l3C-l,2.3,7.8-PeCDF
!3C-2,3.4.7.8-PeCDF
l3C-l,2.3.4,7,8-HxCDF
I3C-1. 2,3.6.7.8 HxCDF
l3C-l.2.3.7.8.9-HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3.4.6.7.8-HpCDF
l3C-l.2.3.4.7.8.9-HpCDF
2000
2000
2000
201)0
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
Pg
1450
1442
1509
1606
1514
2525
1477
1511
1433
1378
1337
1438
1433
1470
1323
ION
R(%) RATIO
73 0.79
72
75
80
76
63 (
74 (
76
72
.53
.24
.25
.03
.87
)78
.60
.55
69 0.52
67 0.51
72 0.51
72 0.52
73 0.43
66 0.44
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200 184
92
B-21
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-06-95
Ext. Date: 12-07-93
Analysis Daw: I5-JAN-96 Time. 18:19:06
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1.2.3,7.8 PeCDD
1. 2.3.4.7.8 H*CDD
1.2.3.6.7.8 HxCDD
l.2.3.7.8.9-HxCDD
1. 2,3,4.6.7,8 HpCDD
OCDD
2.3.7.8TCDF
1.2.3.7.8 PeCDF
2.3.4.7.8 PeCDF
,1.2.3.4.7,8 HuCDF
il. 2. 3.6.7.8 HxCDF
(1.2.3.7.8.9 HxCDF
2.3.4.6.7.8 H»CDF
l.2.3.4.6.7.8-HpCDF
i.2.3.4,7.8.9-HpCDF
OjCDF
[Total Tetra-Furans
Total Tetra Dioxiiu
•Total Penta-Furans
Total Penta Dioxins
total Hexa-Furans
Total Hexa-Dioxins
Total Hepta-Furans
Total Hepu-Dioxins
CONC.
FOUND
36.00
193.90
173.60
140.62
139.06
197.31
368.12
34.94
162.82
169.29
170.26
167.91
176.07
165.92
138.11
169.34
336.43
35.71
36.00
332.11
193.90
680.17
477.83
338.67
233.51
SAMPLE LOWEST
LIMIT OF CALIBRATION ION
DETECTION CONCENTRATIO RATIO
pg/g dry pg/g dry
1.52
7.58
7.58
7.58
7.58
7.58
15.17
1.52
7.58
7.58
7.58
7.58
7.58
7.58
7.58
7.58
15.17
0.77
1.54
1.24
1.27
1.24
1.04
0.88
0.75
1.56
1.56
1.20
1.18
1.20
1.21
1.01
1.01
0.86
0.66
0.77
1.56
1.54
•
1.09
*
1.03
Lab Sample ID: 47482-6-23.S04MSD
Sample Wi/Vol: 6.5930 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A0389IO
Blank Data Filename: A038903
Cal. Ver. Data Filename: A038902
I3C 2.3.7.8-TCDD
l3C-l.2.3.7.8-PeCDD
l3C-1.2.3,4.7.8-HxCDD
I3C-1.2.3.6.7,8 HxCDD
l3C-l.2.3.4,6.7.8-HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-l.2.3,7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3,4,7.8-HxCDF
13C 1.2.3.6.7.8 HxCDF
I3C-I.2.3.7.8.9 IUCDF
!3C-2.3.4.6.7.8-HxCDF
13C-1.2.3.4.6.7.8 HpCDF
l3C-l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD 200
SPIKE
:ONC.
P8
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1398
1273
1426
1585
1436
2548
1362
1334
1274
1321
1276
1417
1425
1376
1198
R(%)
70
64
71
79
72
64
68
67
64
66
64
71
71
69
60
ION
RATIO
0.80
1.52
1.22
1.24
1.04
0.89
0.79
1.57
1.58
0.53
0.30
0.31
0.52
0.44
0.44
172
86
B-22
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-95
Ext. Date: 12-07-93
Analysis Date: I6-MN-96 Time: 11:20:42
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
Lab Sample ID: 47482-6-13. SI5
Sample Wt/Vol: 7.9766 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Auiospec
GC Column ID: 60M DB5
Sample Data Filename: A0390U4
Blank Data Filename: A039003
Cal. Ver. Data Filename: A039002
ANALYTE
'i.
2.3.7.8-TCDD
1.2,3.7.8-PeCDD
j.2.3.4.7.8 HxCDD
1,2.3.6.7.8 HxCDD
i;2.3.7.8.9 HxCDD
l72.3.4.6.7.8-HpCDD
OCDD
2 3.7.8-TCD
I 2.3.7.8-PeCDF
2 3.4.7.8-PeCDF
I 2.3,4.7.8 HxCDF
I 2.3.6,7.8 HxCDF
I 2.3.7.8.9 HxCDF
2.3.4.6.7.8 H»CDF
1,2,3.4.6.7.8 HpCDF
1.2.3.4.7.8.9 HpCDF
OCDF
Total Tetn-Funns
Total Tetra-Dioxins
Total Penta-Funns
Total Penta-Dioxins
Total Hexa-Furans
Total Hexa-Dtoxins
Total Hepta-Furans
Total Hepta-Dioxins
CONC.
FOUND
Pg'gdry
3.46
9.79
9.95
31.83
19.18
572.53
3994.50
(5.19)
7.52
8.21
16.00'
8.82
•
7.98
75.66
3.82
74.74
89.94
51.87
113.25
39.58
105.07
205.82
170.54
1028.51
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION
Pg/g dry Pg'g dry
1.25
6.27
6.27
627
6.27
6.27
12.54
1.25
6.27
6.27
0.34 6.27
6.27
1.01 6.27
6.27
6.27
6.27
12.54
ION
RATIO
0.75
1.67
1.31
1.23
1.29
1.07
0.89
(0.75)
1.50
1.45
*
1.20
•
1.19
1.00
0.97
0.87
0.80
0.77
1.62
1.55
I.II
1.22
•
1.05
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
13C-l,2,3.7.8-PeCDD
13C-1.2.3.4.7.8 HxCDD
I3C-I.2.3.6.7.8 HxCDD
l3C-l,2.3,4,6.7.8-HpCDD
I3C-OCDD
I3C-2.3.7.8 TCDF
l3C-l.2.3.7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
13C-I.2.3.4.7.8 HxCDF
13C-1.2.3.6.7.8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
13C 2,3.4.6.7.8 HxCDF
13C-1,2.3,4.6.7.8 HpCDP
13C 1.2.3.4.7.8.9 HpCDF
CLEANUP STANDARD
37CI-2.3.7.8 TCDD
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUN
Pg
1376
1429
1403
1538
1441
2815
1394
1528
1462
1424
1428
1450
1502
1461
1379
R(%)
69
71
70
77
72
70
70
76
73
71
71
73
75
73
69
ION
RATIO
0.80
.56
.27
.26
.05
088
0.79
.57
.59
0.55
051
052
0.52
0.43
0.42
200
149 74
( ) Second column confirmation not done. 2.3,7.8-TCDF concentration estimated; see teat for detail.
• Analyte not detected.
* Analyte concentration estimated: CDPE
interference, see text for detail.
B-23
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-07-95
Em. Date: 12-07-95
Analysis Date: I6-JAN-96 Time: 12:27:46
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
2.3,7,8-TCDD
l.2.3.7.8-PeCDD
1.2.3.4.7.8 H*CDD
1.2.3.6,7.8-HxCDD
1,2.3.7.8.9 HxCDD
1.2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8-TCDF
1.2,3.7.8-PeCDF
2.3.4.7.8-PeCDF
I.2.3.4.7.8-H»CDF
1.2.3,6,7,8 HxCDF
|,2.3,7.8.9 HxCDP
2,3.4,6.7.8 HxCDF
i;2.3.4.6.7.8 HpCDF
l.2.3.4.7.8.9-HpCDF
OCDF
'I-,.
Total Tetn-Funns
Total Tetra-Dioxins
"folal Penta-Funns
Total Penta-Dtoxins
Total Hexa-Furans
total Hexa Dioxins
Total Hepta-Furans
Total Hepta-Dioxins
CONC.
FOUND
3.33
8.81
9.07
32.10
17.64
591.09
4300.91
(4.91)
8.14
9.35
21.00*
8.23
•
7.91
84.56
3.48
83.05
121.64
44.78
118.08
56.27
115.03
200.08
192.32
1041.07
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO
pg/g dry pg/g dry
1.25
6.23
6.23
6.23
6.23
6.23
12.47
1.25
6.23
6.23
0.34 6.23
6.23
1.02 6.23
6.23
6.23
0.45 6.23
12.47
ION
RATIO
0.74
1.62
1.27
1.20
1.32
1.07
0.88
(0.75)
1.36
1.50
•
I.IS
*
1.19
1.02
0.94
0.86
0.73
0.78
1.61
1.51
1.22
1.23
•
1.06
Lab Sample ID: 47482-6-14. SI6
Sample Wt/Vol: 8.0213 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DBS
Sample Data Filename: A039005
Blank Data Filename: A039003
Cal. Ver. Data Filename: A039002
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
13C-l.2,3.7,8-PeCDD
I3C-I.2.3.4.7.8-HXCDD
l3C-l.2.3.6,7,8-HxCDD
I3C l.2.3.4.6.7.8-HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-l.2.3.7.8-PeCDF
l3C-2.3.4.7.8-PeCDF
l3C-l.2.3,4,7,8-HxCDF
I3C-1. 2.3.6,7.8 HxCDF
l3C-l.2.3.7.8.9-HxCDF
l3C-2.3.4.6.7.8-HxCDF
I3C-I.2.3.4.6.7.8 HpCDF
13C 1.2.3.4.7.8.9 HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
P8
1464
1517
1483
1639
1577
2927
1552
1617
1573
1521
1494
1515
1552
1447
1404
ION
R(X) RATIO
73 0.79
76
74
82
79
73 (
78 (
81
79
.57
.24
.26
.04
)90
).77
59
.61
76 0.52
75 0.51
76 0.52
78 0.52
72 0.43
70 0.42
CLEANUP STANDARD
37CI 2.3,7.8-TCDD
200
161
80
( ) Second column confirmation not done. 2.3.7.8-TCDF concentration estimated; see text for detail.
' Analyte concentration estimated; CDPE interference, see text for detail.
* Analyte not delected.
B-24
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-07-93
EM. Date: 12-12-95
Analysis Date: I6-JAN-96 Time: 13:36:12
Extract Volume (uL): 20
Injection Volume (uL): I
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1.2,3.7.8-PeCDD
1.2.3.4.7.8 HxCDD
1,2.3.6.7.8 HxCDD
1.2,3.7.8.9 HxCDD
1.2.3.4.6.7.8 HpCDD
OCDD
2.3,7.8-TCDF
l.2.3.7.8-PeCDF
2.3.4.7.8-PeCDF
1.2.3.4.7.8 HxCDF
1,2,3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2,3.4.6.7.8 HxCDF
1.2.3.4.6.7.8 HpCDF
l.2.3.4.7.8.9-HpCDF
OCDF
Total Tetn-Funns
Total Tetra Dioxins
Total Penta-Furans
Ton) Penta-Dtoxins
Total Hexa-Furans
Total Hexa-Dioxinj
Total llepta-Furans
Total Hepta-Dioxins
CONC.
FOUND
P8'g dry
4.80
6.31
16.17
9.88
312.06
2273.10
(2.21)
2.99
4.09
3.00'
3.97
•
3.61
34.78
1.90
48.78
36.32
23.78
45.76
22.41
47.36
101.42
96.64
561.94
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO
Pg/g dry pg/g dry
0.40
0.36
ION
RATIO
0.35
0.49
0.22
0.17
0.72
0.36
0.33
1.18
5.88
5.88
5.88
5.88
5.88
11.77
1.18
5.88
5.88
5.88
5.88
5.88
5.88
5.88
5.88
11.77
•
1.67
1.20
1.28
1.31
1.06
0.88
(0.81)
1.66
1.69
•
1.28
*
1.18
1.02
1.07
0.86
0.85
0.74
1.56
1.51
1.23
1.28
Lab Sample ID: 47482-10 2. SIS
Sample Wt/Vol: 8.4973 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A039006
Blank Data Filename: A039003
Cal. Ver. Data Filename: A039002
I3C-2.3.7.8-TCDD
I3C 1.2,3.7.8-PeCDD
13C-1.2.3.4.7.8 HxCDD
I3C 1.2.3,6.7,8-HxCDD
13C-l.2.3.4.6.7,8-HpCDD
I3COCDD
I3C-2.3.7.8-TCDF
!3C-l.2.3.7.8-PeCDF
13C-2.3.4.7.8-PeCDF
l3C-l.2.3.4.7.8-HxCDF
13C 1,2.3.6.7.8 HxCDF
13C 1,2.3.7.8.9 HxCDF
13C 2.3,4.6.7.8 HxCDF
13C 1.2,3.4.6.7.8 HpCDF
I3C l,2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
pg
2000
2000
2000
2000
2000
41)00
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1489
2113
1592
1673
1270
1533
1908
2322
2336
1546
1454
1456
1483
1104
1291
ION
R(%) RATIO
74 0.80
106
80
84
64
38< (
95 (
116
117
.54
.24
.26
.04
).90
).81
.56
.58
77 051
73 0.52
73 052
74 0.52
55 0.44
65 0.44
200
225
113
1.06
() Second column confirmation not done. 2.3.7,8-TCDF concentration estimated; see text for detail.
" Analyte concentration estimated: CDPE interference, see text for detail.
• Analyte not detected.
B-25
-------
PCDD/PCDF ANALYSIS DATA SHEET
Ub Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-95
Ext. Date: 12-12-95
Analysis Date: 16 JAN % Time: 14:42:05
Extnct Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8-TCDD
1.2.3.7.8 PeCDD
1.2.3.4.7.8-HxCDD
1.2.3.6.7.8 HxCDD
1.2.3.7.8.9 HxCDD
1.2.3.4.6.7.8-HpCDD
OCDD
2.3.7.8TCDF
1.2,3.7.8-PeCDF
2.3.4.7.8 PeCDF
I.2,3.4.7.8-HxCDF
1.2.3,6,7.8 HxCDF
1.2,3,7.8.9 HxCDP
2.3.4.6.7.8 HxCDF
i.2.3.4,6.7.8-HpCDF
j.2.3.4.7.8.9-HpCDF
OCDF
Total Tetra-Furans
Tout Tetra Dtoxins
total Penta-Furans
Tgtal Penta-Dioxins
total HcM-Furans
Total Hexa-Dtoxins
Total Hepn-Funns
Total Hepu-Dioxim
CONC.
FOUND
P«'8 dry
0.93
2.69
2.26
3.74
3.86
58.39
615.85
(1.63)
2.22
3.53
3.50'
3.34
*
3.05
21.82
1.62
22.73
30.61
12.73
32.72
18.49
28.14
32.93
49.68
107.20
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry pg/g dry RATIO
0.30
0.71
0.38
028
0.53
0.68
1.03
0.39
0.29
1.12
0.55
0.48
0.38
0.49
0.70
0.55
0.53
0.42
0.35
0.60
2.26
11.32
11.32
11.32
11.32
11.32
22.64
2.26
11.32
11.32
11.32
11.32
11.32
11.32
11.32
11.32
22.64
0.84
1.43
1.24
1.20
1.10
1.03
0.88
(0.73)
1.63
1.46
•
1.14
•
1.23
0.99
1.04
0.84
0.85
0.83
1.48
1.78
1.26
1.22
*
1.04
Lab Sample ID: 47482-10-3. SI9
Sample Wt/Vol: 8.8356 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A039007
Blank Data Filename: A039003
Cal. Ver. Data Filename: A039002
LABELED COMPOUNDS CONC
13C-2.3.7.8TCDD
l3C-1.2.3,7.8-PeCDD
I3C-1.2.3.4.7.8 HxCDD
I3C l.2.3.6.7.8-HxCDD
13C-l,2.3.4.6,7.8-HpCDD
I3C-OCDD
13C-2.3.7.8-TCDF
l3C-l.2.3.7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
!3C-1.2.3.4.7.8-HxCDF
l3C-l.2.3.6.7.8-HxCDF
I3C-I.2.3.7.8.9-IIXCDF
I3C-2.3.4.6.7.8-HXCDF
13C-1.2.3.4.6.7.8 llpCDF
l3C-l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD 200
SPIKE
:ONC.
pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
Pg
1517
1520
1575
1650
1579
2741
1594
1676
1633
1492
1426
1541
1577
1493
1430
R(%)
76
76
79
83
79
69
80
84
82
75
71
77
79
75
71
ION
RATIO
0.78
1.54
1.25
1.24
1.02
0.89
082
1.59
1.58
0.50
O.SI
0.49
0.51
0.44
0.43
218
109
() Second column confirmation not done. 2.3.7.8-TCDF concentration estimated: see text for detail.
* Analyte concentration estimated; CDPE interference. «• • irti for detail.
• Analyte not delected.
B-26
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-07-95
Ext. Date: 12-12-95
Analysis Date: I6-JAN-96 Time: 15:48:21
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
Lab Sample ID: 47482-10-19. S34
Sample Wt/Vol: 7.6565 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Auiospec
GC Column ID: 60M DB5
Sample Data Filename: A039008
Blank Data Filename: A039003
Cal. Ver. Data Filename: A039002
CONC.
ANAI.YTE FOUND
Rg/gdry
2.3.7.8 TCDD 14.62
1.2.3,7.8 PeCDD 84.78
l.2.3.4.7.8-HxCDD 71.47
1.2.3.6,7,8 HxCDD 64.68
1.2,3.7.8,9-HxCDD 96.10
•I.2.3.4,6.7.8 HpCDD 411.19
OCDD 773.32
2.3.7,8-TCDF* 41.85
[J.2.3.7.8-PeCDF 70.83
2.3.4,7.8 PeCDF 99.65
'l.2.3.4.7,8 HxCDF 100.00 '
1.2.3.6.7,8 HxCDF 105.99
1,2.3,7.8.9-HxCDF 5.37
2.3.4,6.7.8 HxCDF 77.02
l.2.3.4.6.7.8-HpCDF 344.45
1.2.3.4.7,8.9 HpCDF 29.80
OCDF 87.93
Total Tetra-Funns 786.22
Total Tetn-Dioxins 425.73
Total Penta-Furans 1010.97
Total Penta-Dioxins 632.56
Total Hexa-Furans 537.05
Total Hexa-Dioxins 748.54
Total Heptt-Furam 494.36
Total Heptt Dfoxins 716.51
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/gdr> pg/gdry RATIO
0.81
2.30
2.61
13.06
13.06
13.06
13.06
13.06
26.12
2.61
13.06
13.06
13.06
13.06
13.06
13.06
13.06
13.06
26.12
0.79
.53
.22
.26
.27
.03
0.89
0.75
.56
.55
•
.15
.39
.07
.00
.04
0.83
0.74
0.75
1.54
1.54
1.20
1.25
•
1.04
I3C-2.3.7.8-TCDD
l3C-1.2.3.7.8-PeCDD
!3C-l.2.3.4.7.8-HxCDD
I3C 1.2.3.6.7.8 HxCDD
l3C-l.2.3.4.6.7.8-HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
I3C-I.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l,2.3.4,7.8-HxCDF
l3C-l.2.3.6.7.8-HxCDF
I3C-I.2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3.4.6.7.8-HpCDF
I3C 1,2.3.4.7.8.9 HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
P8
1623
1518
1628
1855
1798
3247
1657
1631
1604
1534
1530
1696
1600
1722
1605
R(%)
81
76
81
93
90
81
83
82
80
77
77
85
80
86
80
ION
RATIO
0.79
1.55
1.26
1.26
1.04
0.90
0.79
1.57
1.59
0.52
0.52
0.50
0.52
0.45
0.44
200
223
112
f 2,3,7.8-TCDF value from second column confirmation.
" Analyte concentration estimated: CDPE interference, see text for detail.
* Analyte not delected.
B-27
-------
PCOD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-93
Ext. Dale: 12-12-95
Analysis Date: I6-MN-96 Time: 16:55:40
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
CONC.
ANALYTE FOUND
pg/g dry
2.3.7.8-TCDD 45.57
1.2,3.7.8 PeCDD 233.48
1,2.3.4.7.8 HxCDD 212.73
1.2.3.6.7.8 HxCDD 201.38
1.2.3.7.8.9 HxCDD 313.61
1,2.3.4.6.7,8 HpCDD 597.88
OCDD 1058.34
2.3.7.8-TCDF 202.97
1.2,3.7.8 PeCDF 174.41
2.3.4.7.8 PeCDF 228.11
1,2,3.4.7.8 HxCDF 244.72
1,2.3.6.7,8-HxCDP 241.33
1,2.3.7.8.9 HxCDF 149.02
2.3.4.6,7.8 H»CDF 212.90
1.2,3.4.6.7.8 HpCDF 510.32
1.2,3.4.7,8.9 HpCDF 164.88
OCDF 332.72
Total Tem-Furans 977.98
foul Tetra Dioxinj 523.46
Total Pema-Furans 1269.31
Total Pema Dtoxini 987.36
Total Hexa-Furans 1242.53
Total Hexa-Dioxins 1351.72
Total Hepta-Furan$ 811.74
Total Hepta-Dwxim 950.77
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry Pg/g dry RATIO
2.60
13.00
13.00
13.00
13.00
13.00
25.99
2.60
13.00
13.00
13.00
13.00
13.00
13.00
13.00
13.00
25.99
0.75
1.53
1.25
1.22
1.25
1.07
0.89
0.76
1.68
1.59
1.17
1.19
1.18
1.24
1.03
1.04
0.88
0.75
0.77
1.61
1.35
1.21
1.28
*
1.05
Lab Sample ID: 47482-10-20. S34. MS
Sample Wt/Vol: 7.6950 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
CC Column ID: 60M DBS
Sample Data Filename: A039009
Blank Data Filename: A039003
Cal. Ver. Data Filename: A039002
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
13C-l.2.3.7.8-PeCDD
l3C-l.2.3.4.7.8-HxCDD
I3C 1.2.3.6.7,8 HxCDD
I3C-1.2.3.4,6.7.8 HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-1.2.3.7,8-PeCDF
l3C-2.3.4.7.8PeCDF
!3C-1.2.3.4.7.8-HxCDF
I3C-1.2.3.6.7.8 HxCDF
13C-1.2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
I3C-1,2.3.4.6.7.8 HpCDF
l3C-l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD 200
SPIKE
:ONC
P8
2000
2000
2000
2000
20tX)
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1388
1311
1381
1478
1654
3006
1384
1309
1279
1329
1300
1450
1393
1510
1431
ION
R(%) RATIO
69 0.77
66
69
74
83
75 (
69 (
65
64
.58
.25
.26
.05
).87
).77
.60
.58
66 0.52
65 0.52
73 0.51
70 0.52
76 0.44
72 0.43
187
93
B-28
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-95
Ext. Date: 12-12-95
Analysis Date: 16-MN 96 Time: 18:01:38
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
2ANALYTE
22.3,7.8-TCDD
1,2.3.7.8 PeCDD
M".2;3.4.7,8-HxCDD
1 1. 2,3.6.7.8 HxCDD
*l. 2.3.7.8.9 HxCDD
Ł1.2.3.4.6.7.8 HpCDD
,QCDD
^2.3.7.8-TCDF
1.2,3.7.8-PeCDF
2.3,4.7,8 PeCDP
1.2.3,4.7.8 HxCDF
l.2.3.6.7.8-HxCDF
1. 2.3.7.8.9 HxCDF
2.3.4.6.7,8-HxCDF
1.2.3.4,6.7.8 HpCDF
l.2.3.4.7.8;9-HpCDF
OCDF
Total Telra Furans
Total Tetra-Dioxins
Total Penta-Funns
Total Pema-Dioxins
Total Hexa-Furans
Total Hexa-Dioxins
Total Hepta-Furans
Total Hepta-Dioxins
CONC.
FOUND
46.33
255.46
209.34
172.39
281.64
591.83
1145.12
186.98
181.54
231.60
246.72
261.15
153.39
224.36
490.06
162.78
331.61
91)3.60
491.90
1158.30
884.17
1269.46
1214.11
780.94
917.13
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry pg/g dry RATIO
2.61
13.06
13.06
13.06
13.06
13.06
26.12
2.61
13.06
13.06
13.06
13.06
13.06
13.06
13.06
13.06
26.12
0.79
0.74
1.57
1.50
1.20
1.26
•
1.09
0.77
1.60
1.23
1.26
1.21
1.02
0.87
0.76
1.34
1.58
1.20
1.28
1.18
1.19
1.00
1.00
0.89
0.79
0.74
1.57
I.SO
1.20
1.26
»
1.09
Lab Sample ID: 47482-10-21. S34. MSD
Sample Wl/Vol: 7.6564 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A0390IO
Blank Data Filename: A039003
Cal. Ver. Data Filename: A039002
LABELED COMPOUNDS
I3C-2.3.7.8 TCDD
!3C-l,2.3.7.8-PeCDD
l3C-l.2.3.4.7,8-HxCDD
l3C-l.2.3.6.7.8-llxCDD
1 3C- 1 .2.3,4.6.7.8-llpCDD
I3COCDD
I3C-2.3.7.8-TCDF
13C-1.2.3.7.8-PeCDF
I3C 2.3.4.7.8 PeCDF
l3C-l,2.3,4.7.8-HxCDF
l3C-l.2.3.6.7,8-llxCDF
l3C-l,2.3.7.8.9-HxCDF
l3C-2,3.4.6.7,8-HxCDF
l3C-l.2.3.4.6.7,8-HpCDF
I3C-I.2.3.4.7.8.9 HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2(MX)
2000
4(XK)
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC
FOUN
P8
1190
972
1119
1266
1217
2193
1159
1115
1042
1055
992
1141
1050
1121
1053
ION
R(%) RATIO
59 0.78
49
56
63
61
55 (
58 (
56
52
.53
.25
.26
.05
).87
).78
.59
.57
53 0.51
50 0.51
57 0.51
53 0.52
56 0.44
53 043
CLEANUP STANDARD
37CI-2.3.7.8 TCDD
200
158
79
B-29
-------
PCOD/PCDF ANALYSIS DATA SHEET
Lib Name: BATTELLE
Matrix: SOIL
Simple Receipt Dale: 12-07-95
Exl. Date: 12-12-93
Analysis Date: l7-JAN-96Time: 11:33:14
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: 1:2
Lab Sample ID: 47482-10-22. METHOD
Sample Wt/Vol: 10.0000 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A039I05
Blank Data Filename: A039I03
Cal. Ver. Data Filename: A039I02
ANALYTE
2.3.7.8TCDD
1,2.3.7.8-PeCDD
1.2.3,4.7,8 HxCDD
1.2.3.6.7.8 HxCDD
1.2.3.7.8.9 HxCDD
1.2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8-TCDF
1.2,3.7.8-PeCDF
2.3.4.7.8-PeCDF
,2.3.4.7.8-H»CDF
.2.3.6.7.8 H»CDF
,2.3.7,8.9-HxCDF
.3.4.6.7.8 HxCDF
.2.3.4.6.7.8-HpCDF
.2,3.4.7.8.9 HpCDF
OCDF
Total Tctra-Furans
Total Tetra-Dioxins
Total Pena-Funns
Total Pema-Dioxins
Total Hexa Furans
Total Hexa-Dioxins
Total Hepta-Furans
Total Hepta-Dioxins
SAMPLE LOWEST
CONC. LIMIT OF CALIBRATION
FOUND DETECTION CONCENTRATION ION
Pg/g dry pg/g dry pg/g dry RATIO
1.08
1.34
1.68
1.61
1.57
3.73
45.49"
4.81-
1.62
•
1.57
2.59
1.40
1.92
1.98
1.14
1.74
2.84
2.00
2.44
1.48
1.26
1.78
1.52
2.36
4.00
20.00
20.00
20.00
20.00
20.00
40.00
4.00
20.00
20.00
20.00
20.00
20.00
20.00
20.00
20.00
40.00
LABELED COMPOUNDS
I3C-2.3.7.8 TCDD
13C-1.2.3.7.8 PeCDD
I3C-I.2.3.4.7.8 HxCDD
13C-l.2.3.6.7.8-HxCDD
l3C-l.2.3.4.6.7,8-HpCDD
I3C-OCDD
13C-2.3.7.8-TCDF
13C-1.2.3.7.8 PeCDF
13C-2.3.4.7.8 PeCDF
l3C-l,2.3.4.7.8-HxCDF
l3C-l.2.3.6.7,8-HxCDF
l3C-1.2.3.7.8.9-HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3.4.6.7.8-HpCDF
l3C-l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
CONC.
P8
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
P8
1600
1443
1668
1856
1674
2916
1573
1473
811
1568
1603
1659
1635
1617
1432
ION
R(*> RATIO
80 0.79
72
83
93
84
73 (
79 (
74
41
.58
.25
.26
.00
).88
).82
.60
.56
78 0.56
80 0.49
83 0.51
82 0.49
81 0.44
72 0.44
200
177
88
* Sample limh of detection (LOD) higher than lowest calibration concentration
• Analyte not detected.
B-30
-------
Soil SRM (Simple S02) Recovery Remits:
Soil SRM S02 S02
Analyte Target cone. cone, found % REC
(Pg'g) (Pg/g)
2378-TCDD 500 487 97.4
12378-PeCDD 1000 1072 1072
123478-1 IxCDD 1000 941 941
123678-HxCDD 1000 864 864
123789-HxCDD 1000 927 92.7
1234678-HpCDD 1500 1451 96.7
OCDD 2500 3087 1235
2378-TCDF 500 468 936
12378-PeCDF 1000 925 92.5
23478-PcCDF 1000 972 972
•f ~
ji23478-HxCDF 1000 966 96.6
lj23678-IlxCDF 1000 942 942
i>23789-HxCDF 1000 1011 101.1
234678-1 IxCDF 1000 936 936
1234678-HpCDF 1500 1332 88.8
1234789-HpCDF 1500 1414 94.3
OCDF 2500 2348 93.9
C-4
-------
Detection Limit (DL) Results for S03:
S03 S03DL DL Spike S03 DL
Analyte cone, found cone, found cone. % REC #
(Pg'g) (Pg/g) (Pg/g)
2378-TCDD * 9.6 7.6 1275
12378-PeCDD * 46.4 378 1228
123478-HxCDD 15 40.5 378 1032
123678-HxCDD 1.7 359 37.8 91.0
123789-IIxCDD 2.0 390 37.8 981
1234678-HpCDD 28.0 604 378 91.9
OCDD 285.7 270.8 75.6 75.0
2378-TCDF 1.6 98 7.6 1072
12378-PeCDF 2.0 405 37.8 101.9
23478-PeCDF * 436 378 1154
123478-HxCDF * 408 37.8 107.9
123678-HxCDF 1.3 42.3 37.8 108.2
123789-HxCDF * 42.3 37.8 1120
234678-HxCDF * 40.6 37.8 107.5
1234678-HpCDF 7.4 38.9 37.8 860
1234789-1 IpCDF 1.4 408 378 1042
OCDF 18.3 87.9 75.6 93.6
# Percent recovery calculated using the equation:
% REC = 100 (MS cone. found)/(Spike cone. + Background cone.)
C-5
-------
Matrix Spike/Matrix Spike Duplicate Result* for S04:
Analyte
2378-TCDD
12378-PeCDD
123478-1 IxCDD
123678-HxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
[123478-HxCDF
123678-1 IxCDF
|23789-HxC»F
b,4678-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
S04
cone, found
(Pg/g)
*
*
0.7
14
2.1
316
298.3
*
*
*
•
055A
*
09
65
*
18.0
SIMMS
cone, found
-------
Matrix Spike/Matrix Spike Duplkate Remits for S34:
Analyte
2378-TCDD
12378-PeCDD
123478-HxCDD
123678-1 IxCDD
123789-HxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
123789-HxCDF
234678-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
S34
cone, found
(Pg/g)
14.6
' 84.8
71.5
64.7
96.1
411.2
773.3
152.3
708
99.7
100.00A
106.0
5.4
77.0
344.4
298
87.9
S34MS
cone, found
(Pg'g)
45.6
233.5
212.7
201.4
3136
597.9
10583
203.0
174.4
228.1
244.7
241.3
1490
212.9
510.3
164.9
332.7
S34 MS Dup
cone, found
(Pg/g)
463
255.5
209.3
1724
281.6
591.8
1145.1
187.0
181.5
2316
246.7
261.1
153.4
224.4
490.1
1628
331.6
MS Spike
cone.
(Pg/g)
260
1300
1300
130.0
1300
130.0
259.9
260
1300
130.0
1300
130.0
130.0
130.0
130.0
1300
259.9
MSD Spike
cone.
(Pg/g)
261
1306
1306
1306
130.6
1306
261.2
26.1
130.6
130.6
130.6
130.6
1306
1306
130.6
130.6
261.2
S34MS
•/. REC #
112.2
108.7
105.6
103.5
1387
1105
102.4
113.8
869
99.4
188.3
102.3
1101
102.9
107.6
103.2
95.7
S34 MSD
% REC #
1137
1186
1036
883
124.2
1092
1107
104.8
90.1
1006
1889
110.4
112.8
1081
1032
101.5
95.0
MS/MSD
RPD
1.66
8.99
161
15.51
10.74
1.02
7.88
8.20
4.01
1 51
0.82
7.89
289
5.24
4.05
1.28
0.33
A Analyte concentration estimated; CDPE interference, see text for detail.
# Percent recovery calculated using the equation:
% REC = 100 (MS cone, foundV(Spikc cone. + Background cone.)
C-3
-------
PCDD/PCDP ANALYSIS DATA SHEET
Lab Name: BATTELLE
Mitrix: SOIL
Sample Receipt Dale: 12-08-95
Ext. Date: 12-12-95
Analysis Dale: I8-JAN-96 Time: 19:24:45
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8-TCDD
1.2.3,7.8-PeCDD
1.2.3.4.7.8 HxCDD
J.2.3.6.7,8 HxCDD
(l,2,3.7.8.9 HxCDD
l.2.3.4.6.7.8-llpCDD
bCDD
•2.3.7.8 TCDF*
*r.2.3.7,8-PeCDF
2.3.4.7,8-PeCDF
il.2.3.4.7.8 HxCDF
J.2.3.6.7.8 HxCDF
Ł.2.3.7.8.9 HxCDF
2.3,4.6.7.8 HxCDF
d.2.3.4.6.7.8 HpCDF
1.2.3,4.7,8.9 HpCDF
OCDF
Total Tetra-Furans
Total Tetra-Dioxinj
Total Penta-Furans
Total Penta-Dioxins
Total Hexa-Funns
Total Hexa-Dloxins
Total Hepta-Furans
Total Hepta-Dioxinf
CONC.
FOUND
Pg'gdry
4.15
21.02
18.30
17.54
26.64
130.35
668.85
11.24
17.66
23.94
27.00"
29.92
1.74
22.72
98.58
8.79
42.12
195.58
87.06
238.88
119.68
149.99
192.53
150.98
236.82
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO
pg/g dry pg/g dry
2.50
12.48
12.48
12.48
12.48
12.48
24.%
2.5(1
12.48
12.48
0.53 12.48
12.48
0.63 12.48
12.48
12.48
0.48 12.48
24.%
ION
RATIO
0.66
.42
.20
.29
.16
.06
.87
.79
.46
.44
•
.16
.31
.11
.01
0.93
0.84
0.69
0.81
1.52
1.42
1.13
1.23
•
1.01
Lab Sample ID: 47482 10-18. S33. Duplicate
Sample Wt/Vol: 8.0124 unils: g
Initial Calibration Dale: 04-13-95
Instrument ID: Auiospec
GC Column ID: 60M DB5
Sample Data Filename: A03921I
Blank Data Filename: A039203
Cal. Ver. Data Filename: A039202
LABELED COMPOUNDS
I3C-2.3.7.8 TCDD
!3C-l.2.3.7.8-PeCDD
l3C-l.2.3.4.7.8-HxCDD
l3C-l,2,3.6.7.8-HxCDD
1 3C-1 .2.3.4.6,7.8-llpCDD
I3COCDD
I3C 2.3.7.8 TCDF
I3C-I.2.3.7.8 PeCDF
l3C-2.3.4,7.8-PeCDF
l3C-l,2.3.4.7.8-HxCDF
l3C-l.2.3,6.7.8-HxCDF
l3C-l.2.3.7.8.9-HxCDF
l3C-2.3.4.6.7.8-HxCDF
1 3C-1 ,2,3.4.6.7,8-HpCDF
13C-l.2.3.4.7.8.9-HpCDF
SPIKE
CONC
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUN
Pg
1756
1547
1628
1883
1697
3260
1664
1493
1467
1449
1448
1740
1525
1541
1492
R(%)
88
77
81
94
85
82
83
75
73
72
72
87
76
77
75
ION
RATIO
0.78
1.52
1.32
1.13
1.02
0.89
0.79
1.55
1.57
0.52
0.51
0.52
0.51
0.43
0.42
CLEANUP STANDARD
37CI 2.3.7.8-TCDD
200 220
III)
12.3.7.8-TCDF value from second column confirmation.
* Analyte concentration estimated, CDPE interference, see text Tor detail.
• Analyte not detected.
B-45
-------
ATTACHMENT C - SUMMARY OF LABORATORY QUALITY CONTROL RESULTS
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95
Ext. Date: 12-12-93
Analysis Date: I8-JAN-96 Time: 17:11:56
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
,2.3.7,8-PeCDD
,2,3.4.7.8-HxCDD
,2.3,6,7.8 HxCDD
.2.3,7,8.9 HxCDD
,2,3.4.6.7,8-HpCDD
OCDD
2.3.7.8-TCDF
1.2.3,7.8-PeCDF
2;3.4.7.8-PeCDF
|.?,3.4.7.8-HxCDF
J.2.3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2.3.4.6.7.8-HxCDF
^2.3.4.6,7,8-HpCDF
j.2.3.4.7,8.9 llpCDF
OCDF
Lab Sample ID: 47482-10-16. S32
Sample Wt/Vol: 10.0644 units: ;
Initial Calibration Date: 04-13-95
Instnimenl ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A039209
Blank Data Filename: A039203
Cal. Ver. Data Filename: A039202
Total Ten-
Ton! Tetra
Total Pent*
Total Penta
Total Hexa
Total Hexa
Tout Hepta
Total Hepta
•Furans
Dioxins
•Furans
•Dioxins
•Furans
Dioxins
-Furans
Dioxins
SAMPLE LOWEST
CONC. LIMIT OF CALIBRATION
FOUND DETECTION CONCENTRATION ION
pg/8«lry pg/gdry Pg/g u>y RATIO
0.57
1.25
0.52
0.34
0.41
0.%
28.06'
0.30
1.67
0.95
0.46
0.41
0.54
0.77
0.74
0.41
0.91
0.62
0.55
1.20
1.51
0.58
0.61
0.83
0.96
1.99
9.94
9.94
9.94
994
9.94
19.87
1.99
994
9.94
9.94
9.94
9.94
9.94
9.94
9.94
19.87
LABELED COMPOUNDS
13C-2.3.7.8-TCDD
l3C-l,2.3.7.8-PeCDD
l3C-l,2,3.4.7.8-HxCDD
l3C-l.2.3.6.7.8-HxCDD
l3C-l.2,3.4.6.7.8-HpCI)D
I3COCDD
I3C-2.3.7.8-TCDF
!3C-1.2.3.7.8-PeCDF
I3C 2.3.4.7.8 PeCDF
I3C-I.2.3.4.7.8 HxCDF
I3C 1.2.3.6.7.8 HxCDF
l3C-l,2.3.7.8.9-llxCDF
I3C-2.3.4.6.7.8 HxCDF
1 3C- 1 ,2.3.4.6.7.8-HpCDF
1 3C- 1 ,2.3,4.7.8.9-HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2INX)
2(XK)
4000
2000
2000
2(XK)
2000
2000
2000
21)00
2000
2000
CONC.
FOUND
Pg
1449
1255
1435
1804
1449
2606
1362
1298
1292
1316
1390
1441
1375
1326
1282
72
63
72
90
72
65
68
65
65
66
69
72
69
66
64
ION
RATIO
0.79
1.50
1 20
1 24
1 04
0.89
0.78
1.58
1.59
0.53
0.51
0 50
0.52
0 43
0.43
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
192
" Sample limit of detection (LOD) higher man lowest calibration concentration.
• AnalyK not detected.
B-43
-------
PCDO/PCDF ANALYSIS DATA SHEET
Lab Nime: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95
Ext. Date: 12-12-95
Analysis Date: 18-JAN-96 Time: 18:17:54
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8-TCDD
1.2.3.7.8 PeCDD
1.2.3.4.7.8-HxCDD
1.2.3.6.7.8 HxCDD
1.2.3,7,8.9-HxCDD
1.2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8-TCDFI
1.2,3.7.8-PeCDF
2.3.4.7.8 PeCDF
l.2.3.4.7.8-HxCDF
1.2.3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2.3.4.6,7.8 HxCDF
1.2.3.4.6.7,8 HpCDF
1.2,3,4.7,8.9-HpCDF
OCDF
Total Tetra-Furans
Total Tetra-Dloxins
•Total Pema-Furans
•total Penta Dioxini
Toul Hexa-Furans
•Total Hexa-Dioxins
Total Htpu-Furans
Total Hepta-Dioxins
CONC.
FOUND
pg/g dry
4.20
21.52
20.61
18.15
2669
139.24
653.25
11.40
20.11
26.55
37.00-
31.68
1.79
26.13
106.75
9.30
44.74
195.62
105.97
254.09
134.88
142.44
215.79
165.87
255.32
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO ION
pg/g dry pg/g dry RATIO
0.61
0.73
0.59
2.50
12.52
12.52
12.52
12.52
12.52
25.04
2.50
12.52
12.52
12.52
12.52
12.52
12.52
12.52
12.52
25.04
0.76
.60
.18
.19
.20
.04
0.88
0.82
.46
.47
•
.18
.08
.18
.01
.01
0.84
0.81
0.74
1.45
1.59
1.18
1.23
•
1.08
Lab Sample ID: 47482-10 17. S33
Sample Wl/Vul: 7.9871 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A0392IO
Blank Data Filename: A039203
Cal. Ver. Data Filename: A039202
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
l3C-l,2.3.7.8-PeCDD
l3C-l,2.3,4.7,8-HxCDD
l3C-1.2.3.6,7.8-HxCDD
l3C-1.2.3.4.6.7.8-HpCDD
I3COCDD
I3C-2.3.7.8TCDF
13C-l,2.3.7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3.4.7,8-HxCDF
I3C-1. 2.3.6,7.8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
!3C-2.3.4.6.7.8-HxCDF
1 3C-1 .2.3.4.6.7.8-HpCDF
13C-l.2.3.4.7.8.9-HpCDF
SPIKE
CONC
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1075
980
941
1197
1025
2137
1000
949
914
924
925
1075
933
923
922
54
49
47
60
SI
53
50
47
46
46
46
54
47
46
46
ION
RATIO
0.79
1.58
1.22
1.25
1 02
0.87
0.77
1.56
1.60
0.51
0.51
0.52
0.53
0.44
0.43
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
139
70
12.3,7.8-TCDF value from second column confirmation.
* Analyte concentration estimated; CDPE interference, see text for detail.
* Analyte not detected.
B-44
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lib Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95
Ext. Date: 12-12-93
Analysis Date: I8-JAN-96 Time: 14:55:00
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
Lab Sample 1D:47482-IO 14. S30
Sample Wt/Vol: 8.0175
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A039207
Blank Data Filename: A039203
Cal. Ver. Data Filename:
units: g
ANALYTE
2.3,7.8-TCDD
1.2.3.7,8-PeCDD
1.2,3,4.7.8 HxCDD
1.2,3.6.7.8 llxCDD
1.2,3.7.8.9 HxCDD
1.2.3.4,6.7.8 HpCDD
OCDD
2.3.7.8TCDFf
1.2.3,7.8-PeCDF
2,3.4.7.8 PeCDF
1.2.3.4.7.8 HxCDF
1.2.3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2.3.4.6.7,8 HxCDF
l.2.3.4.6.7.8-HpCDF
l.2.3.4.7.8.9-HpCDF
OCDF
Total Tetra-Furans
Total Tetra-Dioxins
Tout Penta-Furans
Total Penta-Dioxins
Total Hexa Furans
Total Hexa-Dioxins
Total Hepta-Furans
Total Hepta-Dtoxins
CONC.
FOUND
P8/8 dry
56.99
393.18
297.59
295.49
422.85
1508.86
2581.50
184.66
298.89
434.37
420.00-
437.19
24.16
327.62
1340.60
123.81
307.96
3517.40
1839.01
4422.76
3037.44
2024.89
3078.33
1927.79
2683.34
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry pg/g dry RATIO
0.41
2.49
12.47
12.47
12.47
12.47
12.47
24.95
2.49
12.47
12.47
12.47
12.47
12.47
12.47
12.47
12.47
24.95
0.76
.57
.22
.25
.24
.06
0.89
0.75
.58
.54
•
.15
.23
.18
.01
.01
0.85
0.72
0.76
1.53
1.47
1.38
1.24
•
1.04
I3C-2.3.7.8-TCDD
13C 1.2.3.7.8-PeCDD
l3C-l.2.3.4.7,8-HxCDD
I3C-1.2.3.6.7,8 llxCDD
I3C 1,2,3,4.6.7.8-llpCDD
I3COCDD
I3C-2.3.7.8-TCDF
I3C 1.2.3.7.8 PeCDF
13C 2.3.4.7.8 PeCDF
l3C-l.2.3.4,7,8-HxCDF
I3C-I.2.3.6.7.8 HxCDF
13C 1.2.3.7,8.9 HxCDF
13C 2.3.4,6.7.8 HxCDF
l3C-l.2.3.4.6.7.8-llpCDF
13C-1.2.3.4.7.8.9 HpCDF
CLEANUP STANDARD
37CI 2.3,7.8-TCDD
SPIKE
:ONC.
pg
2000
2000
2000
2
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Dale: 12-08-95
Exi. Date: 12-12-93
Analysis Dale: l8-JAN-96Time: 16:01:00
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1.2.3.7,8-PeCDD
l.2.3.4.7.8-HxCDD
1.2.3,6.7.8 HxCDD
1.2,3.7.8.9 HxCDD
1.2.3,4.6,7,8-HpCDD
OCDD
2.3.7.8-TCDF*
1.2.3.7.8 PeCDF
2.3.4.7.8-PeCDF
1.2,3,4.7.8-HxCDF
1.2.3.6.7.8 HxCDF
1,2.3.7,8.9-HxCDF
2.3.4.6.7.8-HxCDF
1.2.3.4.6.7.8 HpCDF
1.2.3.4.7.8.9-HpCDF
OCDF
Total Tetn-Furans
Total Tetra-Dioxins
Total Pema-Furans
Total Penta-Dioxins
Total Hexa-Furans
Total Hexa-Dioxins
Total Hepia-Funns
Total Hepta-Dioxins
CONC.
FOUND
pg/gdry
72.54
405.88
358.99
305.24
462.25
1634.40
2662.38
208.93
337.39
486.79
460.00*
530.30
26.25
375.89
1435.59
130.35
300.56
4219.69
2034.88
4797.72
2530.19
2635.91
3495.62
2036.93
2834.56
SAMPLE LOWEST
LIMFT OF CALIBRATION
DETECTION O
pg/gdry
0.44
ENTRATION ION
ig/g dry RATIO
2.45 0.77
12.24
12.24
12.24
12.24
12.24
24.48 (
2.45 (
12.24
12.24
12.24
12.24
12.24
12.24
12.24
12.24
.54
.25
.27
.28
.07
).89
).77
.50
.55
*
.21
.18
.24
.01
.01
24.48 0.88
0.74
0.77
1.54
1.44
1.18
1.26
Lab Sample ID: 47482-10-15. S31
Sample Wt/Vol: 8.1683 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DBS
Sample Dau Filename: A039208
Blank Dau Filename: A039203
Cal. Ver. Data Filename. A039202
LABELED COMPOUNDS CONC
I3C-2.3.7.8-TCDD
l3C-l.2.3.7.8-PeCDD
13C-1.2.3.4,7.8 HxCDD
I3C-I.2.3.6.7.8 HxCDD
13C-1.2.3.4.6.7.8 HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
13C-1.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
)3C-l.2.3.4.7.8-HxCDF
13C-1.2.3.6.7.8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
I3C-1.2.3.4.6.7.8 HpCDF
13C 1.2.3.4.7.8,9 HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
:ONC.
pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUN
P8
1760
1738
1702
2023
1723
2793
1818
1764
1752
1756
1756
1700
1804
1621
1503
R(%)
88
87
85
101
86
70
91
88
88
88
88
85
90
81
75
ION
RATIO
0.79
1.53
1.24
1.27
1.05
0.87
0.78
1.60
1.62
0.52
O.SI
0.52
0.52
0.42
0.43
200
242
121
1.06
12.3.7,8-TCDF value from second column confirmation.
* Analyte concentration estimated; CDPE interference, sec text for detail.
* Analyte not detected.
B-42
-------
PCOD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95
Ext. Date: 12-12-95
Analysis Date: 18-MN 96 Time: 12:37:55
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8-TCDD
l.2.3.7.8-PeCDD
1.2.3,4.7.8 HxCDD
1.2.3.6.7.8 HxCDD
1,2.3,7.8.9 HxCDD
1,2.3,4.6.7,8 HpCDD
OCDD
2,3.7,8-TCDFiT
1.2,3.7.8-PeCDF
2.3,4.7.8 PeCDF
1.2.3.4.7.8 HxCDF
1.2.3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2,3.4.6.7.8 HxCDF
i.2.3.4.6.7.8-HpCDF
U.3.4,7.8.9-HpCDF
bCDF
•*•
Total Tetn Furans
Total Telra-Dioxins
Total Penta-Furans
Total Penta-Dioxins
Total Hexa-Furans
Total Hexa-Dioxins
Total Hepta-Furans
Total Hepta-Dioxins
CONC.
FOUND
pg/gdry
4.71
24.62
21.94
29.91
36.29
482.26
4811.18
10.66
18.51
26.61
34.00'
28.13
1.98
20.43
138.76
11.10
199.37
244.29
115.10
278.91
161.29
188.32
278.57
322.68
843.23
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION
pg/g dry pg/g dry
2.38
11.90
11.90
11.90
11.90
11.90
23.80
2.38
11.90
11.90
0.34 11.90
11.90
0.44 11.90
11.90
11.90
0.32 11.90
23.80
ION
RATIO
0.75
.56
.32
.33
.28
.08
.89
.82
.53
.72
*
.31
.37
.21
.03
0.98
0.88
0.81
0.79
1.55
1.57
1.18
1.26
*
1.08
Lab Sample ID: 47482-10-12. S28
Sample Wt/Vol: 8.4043 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A039205
Blank Data Filename: A039203
Cal. Ver. Data Filename: A039202
LABELED COMPOUNDS
I3C-2.3.7.8-TCDD
l3C-l.2,3.7.8-PeCDD
l3C-i.2.3.4.7.8-HxCDD
l3C-l.2.3,6,7.8-HxCDD
l3C-l.2.3.4.6.7.8-HpCDD
I3C-OCDD
13C-2.3.7.8-TCDF
l3C-1.2,3.7.8-PeCDF
!3C-2.3.4.7.8-PeCDF
13C-l.2.3.4,7.8-HxCDF
13C 1.2.3.6.7.8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
l3C-2.3.4.6.7.8-HxCDF
13C 1.2.3.4.6,7.8 HpCDF
I3C l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
20DO
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1704
1807
1596
1833
1588
3046
1760
1845
1760
1614
1578
1716
1664
1550
1530
ION
R(%) RATIO
85 0.80
90
80
92
79
76 (
88 (
92
88
.55
.23
.24
.04
.88
).79
.58
.59
81 0.52
79 0.52
86 0.52
83 0.51
77 043
76 0.43
200
235 117
12,3.7,8-TCDF value from second column confirmation.
* Analyte concentration estimated: CDPE interference, see text for detail.
* Analyte not detected.
B-39
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Nune: BATTELLE
Matrix: SOIL
Sample Receipt Dace: 12-08-95
EM. Date: 12-12-95
Analysis Dale: I8-1AN-96 Time: 13:49:28
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
CONC.
ANALYTE FOUND
pg/gdry
2.3,7.8-TCDD 38.27
1.2.3,7.8-PeCDD 220.55
1.2.3.4.7,8 HxCDD 179.48
1,2.3.6.7.8 HxCDD 172.87
1.2.3.7.8.9 HxCDD 260.79
1.2.3.4.6.7,8 HpCDD 1001.35
OCDD 1973.49
2.3.7.8-TCDF* 105.66
1.2.3.7.8 PeCDF 168.48
2.3,4.7,8-PeCDF 239.20
I.2.3.4.7.8-H»CDF 230.00'
1.2.3.6.7.8 HxCDF 261.58
1.2.3.7.8.9 HxCDF 14.88
2.3.4.6.7.8 HxCDF 195.87
1.2,3.4.6.7.8 HpCDF 772.00
1.2,3.4.7.8.9 HpCDF 68.64
OCDF 297.35
Total Tetra-Furans 2171.82
Total Tetra-Dioxins 1101.21
. Total Penta-Furans 2304.49
total Penta Dioxins 1825.92
Total Hexa Furans 1078.75
foul Hexa Dioxins 1893.64
Total Ilepta-Furans 1184.23
Total Hepta-DJoxins 1779.71
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION
pg/g dry pg/g dry
2.42
12.12
12.12
12.12
12.12
12.12
24.24
2.42
12.12
12.12
0.36 12.12
12.12
12.12
12.12
12.12
12.12
24.24
ION
RATIO
0.75
.60
.33
.17
.21
.05
0.88
0.78
.53
.56
*
.23
.27
.22
.00
.01
0.87
0.76
0.77
1.60
1.44
1.27
1.23
•
1.05
Lab Sample ID: 47482-10-13. S29
Simple Wt/Vol: 8.2512 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A039206
Blank Data Filename: A039203
Cal. Ver. Data Filename: A039202
LABELED COMPOUNDS
13C-2.3.7.8TCDD
!3C-l.2.3.7.8-PeCDD
1 3C-1 ,2.3,4.7.8-HxCDD
I3C-1, 2.3,6.7, 8 HxCDD
I3C 1.2.3,4.6.7.8 HpCDD
I3COCDD
I3C-2.3.7.8-TCDF
13C-1.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3,4.7.8-HxCDF
I3C-I.2.3.6.7.8 HxCDF
l3C-l.2.3.7.8.9-HxCDF
13C-2.3.4.6.7.8-HxCDF
I3C 1.2.3.4.6.7,8 HpCDF
I3C l.2.3.4.7,8.9-HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
P8
1652
1524
1530
1789
1572
3077
1577
1617
1595
1519
1515
1651
1615
1489
1441
83
76
76
89
79
77
79
81
80
76
76
83
81
74
72
ION
RATIO
0.78
1.55
1 27
1 27
1.03
0.89
0.80
1.60
1.57
0 55
0.50
0 53
051
0.44
0.44
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
234 117
12.3.7.8-TCDF value from second column confirmation.
* Analyie concentration estimated; CDPE interference, see text for detail.
* Analyie not detected.
B-40
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95 .
Ext. Date: 12-12-95
Analysis Date: 17-JAN 96 Time: 19:26:41
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1.2,3.7,8 PeCDD
1.2,3.4,7.8-HxCDD
1.2.3,6.7.8 HxCDD
1.2.3,7,8,9 HxCDD
1.2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8TCDF
1.2.3,7.8-PeCDF
2.3.4.7.8-PeCDF
l.2.3.4.7.8-HxCDF
1.2.3.6,7,8-HxCDF
P.2.3.7.8.9 HxCDF
i.3.4.6.7.8 HxCDF
l.2.3.4.6.7.8-HpCDF
i.2.3,4.7.8.9 HpCDF
OCDF
Total Tetra
Total Tetra
Total Penta
Total Penta
Total Hexa
Total Hexa
Total Hepta
Total llepta
Furans
Dioxins
•Furans
•Dioxins
Furans
Dioxins
Furans
Dioxins
CONC.
FOUND
pg/gdry
6.86
17.31
15.18
40.17
36.59
902.55
6995.43
(9.39)
15.48
19.38
36.W
21.26
•
18.87
115.09
15.05
127.34
102.95
180.85
207.96
•
125.37
44.32
274.56
1664.02
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION
pg/g dry pg/g dry
3.03
15.15
15.15
15.15
15.15
15.15
30.31
3.03
15.15
15.15
15.15
15.15
15.15
15.15
15.15
15.15
30.31
1.80
1.16
2.33
ION
RATIO
0.84
1.66
1.21
1.29
1.25
1.06
0.88
(0.84)
1.41
1.45
»
I.II
•
1.22
1.01
1.07
0.85
0.75
0.75
1.52
•
1.18
1.28
»
1.07
Lab Sample ID: 47482-10-10. S26
Sample Wt/Vol: 6.5986 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A039112
Blank Data Filename: A039I03
Cal. Ver. Data Filename: A039I02
LABELED COMPOUNDS
I3C-2.3.7.8 TCDD
!3C-l.2.3.7.8-PeCDD
l3C-l,2.3.4.7.8-HxCDD
I3C-I.2.3.6.7.8-HXCDD
I3C-1. 2.3.4.6.7.8 HpCDD
I3C-OCDD
I3C-2.3.7.8 TCDF
I3C-1. 2.3,7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l,2.3.4.7.8-HxCDF
!3C-l.2.3.6,7.8-HxCDF
l3C-l.2.3.7.8.9-HxCDF
l3C-2.3.4.6.7.8-HxCDF
1 3C-1 .2.3.4.6.7.8-HpCDF
I3C 1.2.3.4.7.8.9 HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1608
1554
1557
1708
1604
2995
1653
1659
1571
1571
1527
1617
1618
1464
1458
R(%)
80
78
78
85
80
75
83
83
79
79
76
81
81
73
73
ION
RATIO
0.82
1.57
1 24
1 25
1.05
0.90
078
1 64
1.59
0 53
0 SI
0 51
0 51
0 44
0.44
CLEANUP STANDARD
37CI-2.3.7.8 TCDD
200
291
145
( ) Second column confirmation not done. 2.3,7.8-TCDF concentration estimated; see text for detail.
" Analyte concentration estimated; CDPE interference, see text for detail.
• Analyte not detected.
B-37
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95
Exl. Date: 12-12-95
Analysis Date: 18-JAN-96 Time: 11:30:40
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
Lab Sample ID: 47482-10-11. S27
Sample Wt/Vol: 7.4S62 units: g
Initial Calibration Dale: 04-I3-9S
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A039204
Blank Data Filename: A039203
Cal. Ver. Data Filename: A039202
ANALYTE
2.3.7.8TCDD
l.2.3.7.8-PeCDD
1,2,3.4.7.8 HxCDD
1,2,3.6.7.8 HxCDD
1.2.3.7.8.9 HxCDD
1.2.3.4,6.7,8 HpCDD
OCDD
2.3.7.8-TCDFf
1.2,3.7.8-PeCDF
2.3,4.7.8-PeCDF
1.2.3.4,7.8 HxCDF
1,2.3.6,7.8-HxCDF
1.2.3.7.8.9 HxCDF
2,3.4.6,7,8 HxCDF
1.2.3,4,6.7,8 HpCDF
l.2.3.4.7.8.9-HpCDF
OCDF
Total Tetra-Furans
Total Tetra-Dtoxins
Total Penta-Furans
Total Penta-Dioxint
Total Hexi-Furans
Total Hexa-Dioxins
Total Hepta-Furans
Total Hepta-Dioxins
CONC.
FOUND
16.91
14.76
19.47
21.65
298.28
2690.97
10.35
14.15
23.17
27.00'
25.99
1.42
20.79
95.99
7.05
61.79
156.51
48.78
202.33
57.25
127.49
183.13
168.95
525.38
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
Pg/g ^ Pg/g dry RATIO
1.52
0.62
0.74
0.54
2.68
13.41
13.41
13.41
13.41
13.41
26.82
2.68
13.41
13.41
13.41
13.41
13.41
13.41
13.41
13.41
26.82
.69
.28
.33
.18
.06
0.88
0.77
.76
.73
•
.18
.09
.23
0.96
0.92
0.92
0.80
0.85
1.48
1.66
1.37
1.20
0.92
1.07
LABELED COMPOUNDS
I3C-2.3.7.8 TCDD
13C-l.2.3.7.8-PeCDD
!3C-1.2.3.4.7.8-HxCDD
13C-1.2.3.6,7.8-HxCDD
13C-l.2.3.4.6.7.8-HpCDD
I3C-OCDD
13C-2.3.7.8-TCDF
!3C-1.2.3.7.8-PeCDF
l3C-2.3.4.7.8-PeCDF
l3C-l,2.3.4,7.8-HxCDF
I3C-1.2.3.6.7.8-HXCDF
l3C-l.2.3.7.8.9-HxCDF
l3C-2.3.4.6.7.8-HxCDF
I3C-1. 2.3.4.6.7.8 HpCDF
I3C l.2.3.4.7.8.9-HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2(NX>
2(KM)
2000
2000
CONC.
FOUND
Pg
1721
1645
1644
1709
1636
2993
1780
1684
1465
1586
1509
1707
1597
1518
1423
1
R(%) RJ
86 (
82
82
85
82
75 (
89 (
84
73
79 <
75 (
85 1
80 1
76 I
71 (
ON
vno
).80
.57
.22
.24
.02
)89
).77
.60
.59
1.50
).49
J.52
J.52
).44
).44
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
231
116
12,3,7,8-TCDF value from second column confirmation.
* Analyte concentration estimated: CDPE interference, see text fordcuu.
* Analytt not delected.
B-38
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95
Ext. Date: 12-12-95
Analysis Date: 17-JAN 96 Time: 17:10:51
Extnct Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1,2.3,7.8 PeCDD
1,2.3.4.7,8-HxCDD
1,2.3.6.7.8 HxCDD
1,2.3,7.8,9 HxCDD
1.2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8-TCDF
I.2.3.7.8-PeCDF
2.3.4.7.8 PeCDF
1.2.3.4.7.8 HxCDF
1.2.3,6,7,8 HxCDF
1,2,3.7.8.9-HxCDF
2.3.4.6.7,8 HxCDF
j',2.3.4.6.7.8 HpCDF
1,2.3.4.7.8,9 HpCDF
OCDF
Total Tetn-Funns
Total Tetn-Dioxins
Total Penta-Furans
Total Penta-Dioxini
Total Hexa-Furans
Total Hexa-Dfoxins
Total Ilepta-Furans
Total Hepca-Dioxins
CONC.
FOUND
Pg/g dry
1.82
2.17
1.76
6.56
4.93
147.41
1892.40
(1.29)
4.W
2.58
13.53
0.98
13.16
18.32
12.98
24.64
7.23
19.92
53.06
29.86
262.01
SAMPLE LOWEST
LIMFT OF CALIBRATION
DETECTION CONCENTRATION
pg/g dry pg/g dry
0.55
I.SO
1.25
I 32
1.23
1.53
2.32
1.43
2.42
I.II
1.63
1.80
0.93
1.25
2.77
13.84
1384
13.84
13.84
13.84
27.69
2.77
13.84
13.84
13.84
13.84
13.84
13.84
13.84
13.84
27.69
Lab Sample ID: 47482-10-8. S24
Sample Wi/Vol: 7.2232 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DBS
Sample Data Filename: A039110
Blank Data Filename: A039I03
Cal. Ver. Data Filename: A039I02
ION
RATIO
0.73
1.60
1.40
1.06
1.13
1.05
0.86
(0.76)
1.14
0.90
1.00
0.86
0.65
0.77
1.71
1.39
1.34
1.18
1.00
1.09
LABELED COMPOUNDS
I3C 2,3.7.8-TCDD
I3C-I.2.3.7.8 PeCDD
l3C-l.2,3.4.7.8-HxCDD
I3C-I.2.3.6.7.8-IUCDD
1 3C- 1 ,2,3.4.6,7.8-HpCDD
I3C-OCDD
I3C-2.3.7.8-TCDF
l3C-1.2.3.7,8-PeCDF
I3C-2.3.4.7.8 PeCDF
l3C-l.2.3.4.7.8-HxCDF
I3C-I.2.3.6.7.8-IUCDF
I3C-1. 2.3.7.8.9 HxCDF
I3C-2.3.4.6.7.8 HxCDF
1 3C- 1 .2.3.4 ,6.7.8-HpCDF
I3C 1.2.3.4.7.8.9 HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
201)0
2000
4000
2000
2000
2000
2000
2000
20(10
2000
2000
2000
CONC.
FOUND
Pg
1447
1384
1441
1434
1327
2503
1398
1374
1337
1168
1175
1411
1220
1147
1139
1
R(%) R>
72 (
69
72
72
66
63 (
70 (
69
67
58 (
59 <
71 1
61 (
57 (
57 t
ON
vno
)80
.54
.24
26
.03
)89
).78
.59
.58
).52
)52
).S2
J.53
>.43
1.44
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
190 95
() Second column confirmation not done. 2.3.7.8-TCDF concentration estimated; see text for detail.
* Analyte concentration estimated; CDPE interference, see text for detail.
• Analyte not detected.
B-35
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-08-95
Ext. Date: 12-12-95
Analysis Date: 17-JAN-96 Time: 18:20:42
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
ANALYTE
2.3.7.8TCDD
1,2.3.7.8 PeCDD
l.2.3.4.7.8-HxCDD
1.2.3.6.7.8 HxCDD
1,2.3.7.8.9 HxCDD
1.2.3,4,6.7,8 HpCDD
OCDD
2.3.7.8-TCDF
1,2,3,7,8-PeCDF
2,3.4.7.8-PeCDF
l,2.3.4.7.8HxCDF
1.2.3.6.7.8 HxCDF
1.2.3,7.8.9 HxCDF
2,3.4,6.7.8 HxCDF
l.2.3.4.6.7.8-HpCDF
1.2.3.4.7.8.9 HpCDF
OCDF
Total Tetn-Funns
Total Tetra-Dknins
Total Penta-Furans
Total Peiua-Dioxins
Total Hexa-Funns
Tout Hexa-Dfoxins
Tout HepbJ-Punni
Total Hepta-Dioxliu
CONC.
FOUND
Pg/g dry
3.37
11.53
10.34
13.67
17.81
154.90
1075.87
(7.06)
10.31
14.27
24.00'
17.64
1.07
14.49
74.88
5.95
48.85
120.59
61.09
146.88
12.37
91.20
139.43
127.28
284.29
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry pg/g dry RATIO
1.03
0.87
0.95
0.88
0.77
0.58
2.46
12.30
12.30
12.30
12.30
12.30
24.60
2.46
12.30
12.30
12.30
12.30
12.30
12.30
12.30
12.30
24.60
0.75
.63
.19
.27
.25
.04
0.88
(0.80)
.62
.36
*
.27
.25
.33
.01
0.89
0.89
0.75
0.72
1.34
1.72
1.20
1.24
0.89
1.01
Lab Sample ID: 47482-10-9. S25
Sample Wl/Vol: 8.1293 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A039111
Blank Data Filename: A039I03
Cal. Ver. Data Filename: A039I02
LABELED COMPOUNDS
I3C-2.3.7.8TCDD
I3C-I.2.3.7.8 PeCDD
I3C-I.2.3.4.7.8-HXCDD
!3C-l.2.3.6.7.8-HxCDD
I3C 1.2.3.4 ,6.7.8-HpCDD
I3C-OCDD
13C-2.3.7.8-TCDF
13C-1. 2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
!3C-1.2.3.4.7.8-HxCDF
I3C-I.2.3.6.7.8 HxCDF
!3C-l.2,3.7.8.9-HxCDF
13C-2,3.4.6.7.8-HxCDF
1 3C-1 .2.3.4 .6.7.8-HpCDF
l3C-l.2.3.4.7.8.9-HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1483
1392
I486
1546
1377.
2566
1367
1481
1388
1436
1351
1482
1463
1279
1302
R(%)
74
70
74
77
69
64
68
74
69
72
68
74
73
64
65
ION
RATIO
0.79
1.53
1.23
1.23
1.07
0.89
0.80
1.60
1.61
0.52
051
0.51
0.51
0.44
0.42
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
202
101
(.) Second column confirmation not done. 2,3,7,8-TCDF concentration estimated: see text for detail.
" Analyte concentration estimated; CDPE interference, see text for detail.
• Analyte not delected.
B-36
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lib Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-95
Exl. Date: 12-12-95
Analysis Date: l7-MN-96Time: 14:38:33
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
Lab Sample ID: 47482-10-6. S22
Sample Wt/Vnl: 7.8343 units:
Initial Calibration Dale: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DBS
Sample Data Filename: A039I08
Blank Data Filename: A039I03
Cal. Ver. Data Filename: A039I02
g
CONC.
ANALYTE FOUND
Pg/g dry
2.3.7.8 TCDD 1.76
1.2.3.7.8 PeCDD 2.85
1.2.3.4.7.8 HxCDD 2.73
1.2.3.6.7.8 HxCDD 5.24
1.2.3.7,8.9 HxCDD 4.10
l.2.3.4.6.7,8-HpCDD 76.76
OCDD 572.75
2.3.7.8-TCDF (1.83)
1.2.3.7.8-PeCDF 2.51
2,3.4.7.8 PeCDF 3.84
l.2.3.4.7.8-HxCDF
,1.2.3.6.7.8 HxCDF 3.96
,1.2,3.7.8.9-HxCDF •
,2,3.4.6.7.8-HxCDF 3.36
1.2,3.4.6.7.8 HpCDF 20.18
,'l.2.3.4.7.8,9-HpCDF 1-13
OCDF 11.78
T
.Total Tetra-Funns 34.57
-.Total Tetra-Dioxins 16.54
{Total Penu-Furans 42.43
Total Penta-Dioxins 11.69
Total Hexa Furans 27.88
Total Hexa-Dioxins 41.02
Total Hepta-Furani 40.11
Tout Hepta-Dioxins 138.28
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATIO
pg/g dry pg/g dry
025
0.75
0.67
0.68
0.64
0.72
1.01
0.70
1.17
0.61
0.73
0.48
0.70
2.55
12.76
12.76
12.76
12.76
12.76
25.53
2.55
12.76
12.76
12.76
12.76
12.76
12.76
12.76
12.76
25.53
ION
RATIO
0.69
1.68
1.15
1.28
1.16
1.02
0.88
(0.75)
1.33
1.53
*
1.13
*
1.18
1.03
0.97
0.91
0.68
0.73
1.65
1.66
1.20
1.20
*
1.07
LABELED COMPOUNDS
I3C 2.3.7.8-TCDD
!3C-l.2.3.7.8-PeCDD
l3C-l.2,3.4.7.8-HxCDD
I3C-I.2.3.6.7.8 HxCDD
1 3C- 1 ,2.3.4 ,6.7.8-HpCDD
I3COCDD
I3C 2.3.7.8-TCDF
l3C-l.2.3,7.8-PeCDF
I3C 2.3.4.7.8 PeCDF
l3C-l.2.3.4.7.8-HxCDF
I3C-1, 2,3.6.7,8 HxCDF
l3C-l.2.3.7.8.9-HxCDF
I3C-2.3.4.6.7.8 HxCDF
l3C-l.2.3.4.6,7,8-llpCDF
I3C-1. 2.3.4.7.8.9 HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
P8
1557
1365
1460
1706
1493
2745
1447
1411
1361
1402
1434
1512
1527
1467
1310
ION
R(%) RATIO
78 0.78
68
73
85
75
69 (
72 (
71
68
.52
.22
.21
.05
)89
).78
.55
.60
70 0.52
72 0.51
76 0.53
76 0.52
73 0.44
66 0.45
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
210 105
() Second column confirmation not done. 2.3.7.8-TCDF concentration estimated; see text for detail.
* Analyte concentration not quantified due to CDPE interference: see text.
* Analyte not detected.
B-33
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab N»me: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-95
Ext. Date: 12-12-9]
Analysis Date: I7-MN-96 Time: 16:04:48
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: 1:2
ANALYTE
2.3.7.8TCDD
1.2.3.7,8-PeCDD
1.2.3.4.7,8 HxCDD
1.2.3.6.7.8 HxCDD
1.2.3.7.8.9 HxCDD
1.2.3.4.6.7,8-HpCDD
OCDD
2.3.7,8-TCDF
1.2.3.7,8-PeCDF
2.3.4.7.8-PeCDP
1.2,3.4,7.8-HxCDF
1.2,3.6,7.8-HxCDF
l.2.3.7.8.9-HxCDF
2,3,4,6.7.8-HxCDF
1,2.3.4.6.7.8 HpCDF
l.2.3.4.7.8.9-HpCDF
OCDF
Total Tetra-Furans
Total Tetra-Dioxins
Total Penta-Furans
Total Penta-Dtoxins
Total Hexa-Furaru
Total Hexa-Dioxins
Total Hepta-Funns
Total Hepta-Dioxins
CONC.
FOUND
pg/g dry
30.41
24.49
29.66
1174.14
18875.28
226.39
19.26
422.85
198.25
»
323.36
*
201.39
575.90
882.00
2449.77
Lab Sample ID: 47482-10-7. S23
Sample Wt/Vol: 7.6321 units: g
Initial Calibration Date: 04-13-95
Instrument ID: Aulospec
GC Column ID: 60M DB5
Sample Data Filename: A039I09
Blank Data Filename: A039I03
Cal. Vtr. Data Filename: A039I02
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION
pg'g dry pg/g
-------
PCDD/PCDF ANALYSIS DATA SHEET
Lab Name: BATTELLE
Matrix: SOIL
Sample Receipt Date: 12-07-93
Ext. Date: 12-12-9)
Analysis Date: I7-JAN-96 Time: 12:43:14
Extract Volume (uL): 20
Injection Volume (uL): 0.5
Dilution Factor: NONE
CONC.
ANALYTE FOUND
Pi/8 dry
2,3.7.8-TCDD 31.06
l.2,3.7.8PeCDD 84.70
1.2.3.4.7.8 HxCDD 14.51
1.2.3.6.7.8 HxCDD 74.43
1.2.3.7.8.9 HxCDD 169.09
1.2.3,4.6.7.8 HpCDD 878.03
OCDD 9005.18
2.3.7.8-TCDF (1.53)
1,2.3.7.8-PeCDF •
2,3.4,7,8-PeCDF •
1.2.3.4.7.8 HxCDF
1.2.3.6.7.8 HxCDF 4.04
1.2.3.7.8.9 HxCDF •
2.3.4.6.7.8 HxCDF 3.64
1,2.3.4.6,7,8 HpCDF 37.16
1.2.3,4.7.8.9 HpCDF 2.66
OCDF 79.09
Total Tetra-Furans 16.91
Total Tetra-Dioxini 78.00
Total Penta-Furans 73.89
Total Penta-Dioxins 287.85
Total Hexa-Furans 58.48
Total Hexa Dioxins 1473.65
Total Hepca-Funns 110.03
Total Heptt-Dioxins 2200.80
Lab Sample ID: 47482-10-4. S20
Sample Wl/Vol: 8.7148 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A039106
Blank Data Filename: A039I03
Cal. Ver. Data Filename: A039I02
SAMPLE LOWEST
LIMIT OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry pg/g dry RATIO
2.04
2.96
2.10
3.47
1.67
2.30
1.44
2.29
11.47
11.47
11.47
11.47
11.47
22.95
2.29
11.47
11.47
11.47
11.47
11.47
11.47
11.47
11.47
22.95
0.80
.57
.21
.23
.24
.06
0.88
(0.72)
*
•
*
1.33
•
1.14
0.98
1.15
0.86
0.77
0.72
1.49
1.54
1.25
1.24
*
LABELED COMPOUNDS
I3C-2.3.7.8 TCDD
13C-l.2,3.7.8-PeCDD
13C-l.2.3.4.7.8-HxCDD
13C-l.2.3.6.7.8-llxCDD
l3C-l,2.3.4.6.7.8-HpCDD
I3COCDD
I3C-2.3.7.8-TCDF
l3C-l.2.3.7.8-PeCDF
I3C-2.3.4.7.8 PeCDF
!3C-l.2.3.4,7.8-HxCDF
I3C-1. 2.3.6.7.8 HxCDF
l3C-l,2.3.7.8,9-HxCDF
l3C-2.3.4,6.7.8-HxCDF
1 3C- 1 .2,3.4.6.7.8-HpCDF
l3C-l.2.3.4.7.8.9-HpCDF
SPIKE
CONC.
Pg
2000
2000
2000
2000
201 K)
4000
2000
2000
201 X)
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
567
522
513
620
588
1029
543
558
519
512
525
601
541
481
488
R(%)
28 <
26 <
26 <
29 <
26 <
27 <
28 <
26 <
26 <
26 <
30 <
27 <
24 <
24 <
ION
RATIO
081
1.56
1 28
1 26
1 04
089
0.80
1.57
1.60
0 52
0.52
0 50
0 51
0 44
0.42
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
200
< Outside
73
36 <
1.05
() Second column confirmation not done. 2.3.7.8-TCDF concentration estimated: see text for detail.
* Analyte concentration not quantified due to CDPE interference; see text.
• Analyte not detected.
B-31
-------
PCDD/PCDF ANALYSIS DATA SHEET
Ub Name: BATTELLE
Murix: SOIL
Sample Receipt Date: 12-07-95
Ext. Date: 12-12-95
Analysis Date: l7-MN96Time: 13:51:19
Extract Volume (uL): 20
Injection Volume (uL): O.S
Dilution Factor: NONE
ANALYTE
2.3,7.8-TCDD
l.2.3.7,8PeCDD
1.2.3.4.7.8 HxCDD
1.2,3.6.7.8 HxCDD
1.2.3.7.8.9 MxCDD
1.2.3.4.6.7.8 HpCDD
OCDD
2.3.7.8-TCDF
1.2.3.7.8 PeCDF
2.3.4.7.8 PeCDF
1.2.3.4,7.8 HxCDF
1,2.3.6.7.8 HxCDF
1.2.3.7.8.9 HxCDF
2,3.4.6.7,8 HxCDF
1.2.3.4.6.7,8 HpCDF
l.2.3.4.7.8.9-HpCDF
OCDF
Total Tern-
Total Ten-
Total Perm
Total Penta
Total Hexa-
Total Hexa
Total Hepta
Total Hepta
•Furans
Dioxins
•Furans
•Dioxins
Furans
Dioxins
•Funuis
•Dioxins
CONC.
FOUND
pg/g dry
1.67
1.68
1.62
3.31
14.48
76.61
(1.12)
1.84
2.49
2.40'
2.32
•
2.42
9.28
•
5.03
16.57
5.29
21.38
5.66
6.78
14.54
11.36
27.92
SAMPLE LOWEST
LIMrr OF CALIBRATION
DETECTION CONCENTRATION ION
pg/g dry pg/g dry RATIO
0.46
0.97
1.09
1.06
1.02
1.03
1.34
1.09
1.74
0.93
1.17
1.46
0.77
1.14
2
13
13
13
13
13
26
2
13
13
13
13
13
13
13
13
26
65
.26
.26
.26
.26
.26
.52
65 ((
.26
.26
.26
.26
.26
.26
.26 (
.26
.52 (
(
(
(
*
.53
.09
.47
.10
.02
).86
).82)
.58
.61
*
.05
•
.29
).92
*
).86
).80
).88
.62
.51
.17
.14
).92
.02
Lab Sample ID: 47482-10-5. S2I
Sample Wi/Vol: 7.5419 units: g
Initial Calibration Dale: 04-13-95
Instrument ID: Autospec
GC Column ID: 60M DB5
Sample Data Filename: A039I07
Blank Data Filename: A039I03
Cal. Ver. Data Filename: A039I02
LABELED COMPOUNDS
I3C-2.3.7.8TCDD
13C-1.2,3.7.8 PeCDD
!3C-l.2.3.4.7.8-HxCDD
I3C-I.2.3.6.7.8 HxCDD
I3C 1.2.3.4.6,7.8 HpCDD
I3COCDD
)3C-2.3.7,8-TCDF
I3C-1.2.3.7.8 PeCDF
I3C-2.3.4.7.8 PeCDF
I3C-I.2.3.4.7.8 HxCDF
I3C-1.2.3.6.7.8 HxCDF
I3C-I.2.3.7.8.9 HxCDF
l3C-2.3.4.6.7,8-HxCDF
13C 1.2,3.4.6.7.8 HpCDF
l3C-l.2.3.4.7.8.9-HpCDF
CLEANUP STANDARD
37CI-2.3.7.8-TCDD
SPIKE
CONC.
Pg
2000
2000
2000
2000
2000
4000
2000
2000
2000
2000
2000
2000
2000
2000
2000
CONC.
FOUND
Pg
1140
1177
1078
1353
1186
2143
1184
1138
1233
1113
1193
1259
1177
1045
1040
R(%)
57
59
54
68
59
54
59
57
62
56
60
63
59
52
52
ION
RATIO
0.78
1.60
1.22
1.24
1.04
0.89
0.80
1.63
1.59
0.51
0.50
0.49
0.52
0.44
0.43
200
158 79
() Second column confirmation not done. 2.3.7.8-TCDF concentration estimated; see text for detail.
' Analyte concentration estimated; CDPE interference, see text for detail.
• Analyte not detected.
B-32
-------
Duplicate Sample Results For S09:
S09 S09 Dup
Analyte cone, found cone, found RPD
(Pg/g) (Pg/g) ('/•)
2378-TCDD 05 0.5 9.6
12378-PeCDD 1.7 2.4 352 #
123478-HxCDD 1.5 20 265 #
123678-HxCDD 1.8 2.3 264 #
123789-HxCDD 2.9 42 373 #
1234678-HpCDD 16.6 19.7 16.9
OCDD 815 900 9.9
2378-TCDF * 20 NC
12378-PeCDF 1.6 1.7 7.1
23478-PeCDF 25 3.7 38.3 #
123478-HxCDF 3.00A I.50A •
123678-HxCDF 26 39 40.9 #
123789-IlxCDF * 04 NC
234678-1 IxCDF 2.6 3.4 24.8
1234678-1 IpCDF 115 138 18.0
1234789-HpCDF 0.7 1.0 35.4 #
OCDF 6.8 7.9 15.2
* Analyte peak not detected.
# RPD outside 25% control limit but measurement made at or below the lowest calibration concentration.
A Analyte concentration estimated; CDPE interference, see text Tor detail.
NC - % RPD not calculated due to a non-detect Tor this analyte in S09.
C-6
-------
Duplicate Sample Result* for S33:
Analyte
2378-TCDD
12378-PeCDD
123478-HxCDD
123678-IIxCDD
123789-1 IxCDD
1234678-HpCDD
OCDD
2378-TCDF
12378-PeCDF
23478-PeCDF
123478-HxCDF
123678-HxCDF
123789-HxCDF
234678-HxCDF
1234678-HpCDF
1234789-HpCDF
OCDF
S33
cone, found
(Pg/g)
4.2
215
20.6
18.2
26.7
139.2
653.3
11.4
20.1
266
37.00*
31.7
1.8
261
106.8
93
44.7
S33 Dup
cone, found
(PR/g)
4.2
21.0
18.3
17.5
266
130.3
668.9
11.2
17.7
239
27.00A
299
1.7
22.7
986
88
421
RPD
C/.)
1.2
24
119
34
02
66
2.4
1.4
13.0
103
*
5.7
28
14.0
8.0
5.6
6.0
Analyle peak not detected.
Analyte concentration estimated; CDPE interference, see text for detail.
C-7
------- |