ESL-TR-87-09
ENVIRONMENTAL FATE AND
EFFECTS OF SHALE-DERIVED
JET FUEL
P.M. PRITCHARD, T.P. MAZIARZ, L.H. MUELLER,
A.W. BOURQUIN

U.S. ENVIRONMENTAL PROTECTION AGENCY
ENVIRONMENTAL RESEARCH LABORATORY
GULF BREEZE FL 32561

JUNE 1988

FINAL REPORT

OCTOBER 1984 - MARCH 1986
    APPROVED FOR PUBLIC RELEASE: DISTRIBUTION UNLIMITED
  ENGINEERING & SERVICES LABORATORY
  AIR FORCE ENGINEERING & SERVICES CENTER
  TYNDALL AIR FORCE BASE, FLORIDA 32403

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WORK UNIT
ACCESSION NO.
75
 11. TITLE (Include Security Classification)
  Environmental  Fate and Effects of  Shale-Derived Jet  Fuel
12. PERSONAL AUTHOR(S)
Pritchard, P.H. ; Maziarz, T.P.; Mueller,
13a. TYPE OF REPORT
Final
13b. TIME COVERED
FROMOct 84 ToMar
L.H.; Bourquin, A.W.
86
14. DATE OF REPORT (Year, Month, Day)
June 1988
15. PAGE COUNT
97
 16. SUPPLEMENTARY NOTATION
  Availability of this report is  specified on reverse  of  front cover.
17. COSATI CODES
FIELD
06
07
GROUP
13
03
SUB-GROUP


18. SUBJECT TERMS (Continue on reverse if necessary and identify by block
Biodegradation Shale-Derived Fuel
Jet Fuel
number)
 19. ABSTRACT (Continue on reverse if necessary and identify by block number)
  Tests were conducted to compare  the environmental fate  of shale oil-derived jet fuel
  with that of petroleum-derived jet fuel.  These tests included chemical  characterization
  of the fuels,  and the water-soluble fraction of each  fuel, also measurement of volatiliza-
  tion and biodegradation rates in laboratory systems designed to simulate three disparate
  aquatic environments.  No major  differences in the volatilization and biodegradation rates
  of the two fuels  were found.  Differences in composition were generally  small and should
  not cause the  behavior of the fuels in aquatic environments to differ.
20. DISTRIBUTION /AVAILABILITY OF ABSTRACT
X2 UNCLASSIFIED/UNLIMITED D SAME AS RPT. d DTIC USERS
MICHAEL V. HENLEY
21. ABSTRACT SECURITY CLASSIFICATION
UNCLASSIFIED
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(904) 283-4297
22c. OFFICE SYMBOL
HO AFESC/RDVC
3D Form 1473,  JUN 86
Previous editions are obsolete.
                                SECURITY CLASSIFICATION OF THIS PAGE
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                                 PREFACE
     This report was prepared by the Microblal Ecology and Biotechnology

branch of the U.S. Environmental Protection Agency at Gulf Breeze, FL.

The research was supported by an interagency agreement RW57931194-01-1

through the Air Force Engineering and Services Center, Engineering and

Services Laboratory at Tyndall Air Force Base, FL 32403.  Captain Robert

C. Beggs and Mr. Michael V. Henley served as Project Officers for the

AFESC/RD.

     This report covers work performed between October 1984 and March

1986.

     The authors would like to thank C.R. Cripe, W.T. Gilliam, and E.J.

O'Neill for their analytical support and technical review of this work.

The assistance of M. Woehle, A. Quarles, T. Baker and P. Paradis is

greatly appreciated.  Val Caston is thanked for her typing and editing.

     This report has been reviewed by the Public Affairs Office (PA)  and

is releasable to the National Technical  Information Service (NTIS).  At

NTIS, it will be available to the general public, including foreign

nationals.

     This report has been reviewed and is approved for publication.
MICHAEL V. HENLEY
Project Officer
THOMAS J. WALKER, Lt Col, USAF, BSC
Chief, Environics Division
                                            <-— ^
 3NNETH T. DENBLEYKER, Maj, USAF
Chief, Environmental Sciences Branch
LAWRENCE D. HOKANSON, Colonel, USAF
Director, Engineering and Services
  Laboratory
                                    ill
                      (The  reverse  of  this  page  is  blank)-

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                               TABLE OF CONTENTS








SECTION                                                                     Page



   I   INTRODUCTION 	      1



       A.  OBJECTIVE 	      1




       B.  BACKGROUND 	      1



       C.  SCOPE/APPROACH 	      6






  II   METHODS



       A.  JET FUEL 	      7



       B.  INSTRUMENT CONDITIONS 	      7



       C.  METHOD REFINEMENTS 	      8



           1.  Extraction Procedure 	      8



           2.  Quiescent Bottle Test 	      9




       D.  SAMPLING SITES 	     12



       E.  COMPOSITIONAL ANALYSIS 	     12




           1.  Neat Fuel 	     12



           2.  Water Soluble Fraction 	     14



       F.  TOXICITY TESTS 	     15



       G.  DISSOLVED ORGANIC CARBON 	     15



       H.  JET FUEL EVAPORATION RATES 	     16




 III   RESULTS



       A.  COMPOSITIONAL ANALYSIS 	     17




           1.  Neat Fuel 	     17



           2.  Water Soluble Fraction 	     17



       B.   BOTTLE TEST OPTIMIZATION 	     22



       C.   QUIESCENT BOTTLE  TESTS 	     22




           1.  Range Point  	     22

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                                 TABLE OF CONTENTS

                                    (CONCLUDED)



                                      Title
Section                                                                       Page



             2.  Bayou Chico	„	     38



             3.  Escambia River 	     56



         D.  TOXICITY TESTS 	     56



         E.  DISSOLVED ORGANIC CARBON 	     56



         F.  JET FUEL EVAPORATION RATE 	     76





    IV   CONCLUSIONS	     80



     V   RECOMMENDATIONS ....		     88



         REFERENCES	     90
                                         VI

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                              LIST OF FIGURES





 Figure                           Title                                     Page



 1  Extraction Methodology with 500 mg/n Sediment  	      10



 2  Extraction Methodology with 5,000 mg/x. Sediment  	      11



 3  Silica Gel Fractionation 	      20



 4  Effect of Sediment Concentration 	      23



 5  Total Hydrocarbon Loss in Range Point Bottle Test  	      24



 6  Loss of Ethylcyclohexane and Benzene in Range  Point Test  	      27



 7  Loss of Cyclohexane and Methylcyclohexane in Range Point  Test  	      28



 8  Loss of Methyl benzene and Ethyl benzene in Range  Point Test  	      29



 9  Loss of Isopropylbenzene and jri-Xylene in Range Point Test  	      30



10  Loss of £-Xylene and £-Xylene in Range Point Test  	      31



11  Loss of 1,3,5-Trimethylbenzene and  1,2,4-Trimethylbenzene



    in Range  Point Test 	      32



12  Loss of 1,2,3-Trimethylbenzene and  Indan in Range  Point Test  	      33



13  Loss of Heptane and Octane in Range  Point Test 	      34



14  Loss of Naphthalene in Range Point  Test 	      35



15  Loss of Nonane and Decane in Range  Point Test  	      36



16  Loss of Pentadecane and Hexadecane  in Range Point  Test	      37



17  Decane Mineralization Following Escambia River Test 	      74



18  Toluene Toxicity in Range Point Water 	      75



19  Solubility of Nonane versus DOC	      77



20  Solubility of 1,3,5-Trimethylbenzene versus DOC	      78



21  Jet Fuel  Evaporation Rate 	      79
                                    vii

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                                LIST OF  TABLES





Table                               Title                                     Page




  1  PHYSICAL  CHARACTERISTICS  OF  JET FUEL  	     3



  2  COMPARISON OF  SHALE-DERIVED  JP-4 WITH PETROLEUM-DERIVED  JP-4,



     LITERATURE VALUES	     4



  3  LIST OF  COMPONENT  HYDROCARBON  MONITORED  THROUGHOUT STUDIES  	    14



  4  COMPARISON OF  SHALE-DERIVED  JP-4 WITH PETROLEUM-DERIVED  JP-4,




     ACTUAL VALUES	    18



  5  WATER SOLUBLE-FRACTION  COMPONENTS 	    21



  5a COMPARISON OF  DISAPPEARANCE  RATES IN  STERILE  AND  ACTIVE



     RANGE POINT SYSTEMS	    25



  6  DATA FROM BAYOU CHICO BOTTLE TEST,  STERILE  WATER  WtTH  SJP-4 	    39



  7  DATA FROM BAYOU CHICO BOTTLE TEST,  ACTIVE WATER WITH SJP-4  	    41



  8  DATA FROM BAYOU CHICO BOTTLE TEST,  STERILE  SEDIMENT WITH SJP-4 	    43



  9  DATA FROM BAYOU CHICO BOTTLE TEST,  ACTIVE SEDIMENT WITN  SJP-4  	    45



 10  DATA FROM BAYOU CHICO BOTTLE TEST,  ACTIVE WATER WITH PJP-4  	    47



 11  DATA FROM BAYOU CHICO BOTTLE TEST,  STERILE  WATER  WITH  PJP-4 	    49



 12  DATA FROM BAYOU CHICO BOTTLE TEST,  STERILE  SEDIMENT WITH PJP-4 	    51



 13  DATA FROM BAYOU CHICO BOTTLE TEST,  ACTIVE SEDIMENT WITH  PJP-4  	    53



 14  COMPARISON OF  DEGRADATION RATES IN  THE BAYOU  CHICO TEST  	    55



 15  DATA FROM ESCAMBIA RIVER  BOTTLE TEST, STERILE WATER WITH SJP-4 	    57



 16  DATA FROM ESCAMBIA RIVER  BOTTLE TEST, ACTIVE  WATER WITH  SJP-4  	    59



 17  DATA FROM ESCAMBIA RIVER  BOTTLE TEST, STERILE SEDIMENT WITH SJP-4	    61



 18  DATA FROM ESCAMBIA RIVER  BOTTLE TEST, ACTIVE  SEDIMENT  WITH  SJP-4 	    63




 19  DATA FROM ESCAMBIA RIVER  BOTTLE TEST, ACTIVE  WATER WITH  PJP-4  	    65



 20  DATA FROM ESCAMBIA RIVER  BOTTLE TEST, STERILE WATER WITH PJP-4 	    67



 21  DATA FROM ESCAMBIA RIVER  BOTTLE TEST, STERILE SEDIMENT WITH PJP-4 	    69
                                      viii

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                          LIST OF TABLES (CONCLUDED)

Table                              Title                                     Page

 22  DATA FROM ESCAMBIA RIVER BOTTLE TEST,  ACTIVE  SEDIMENT  WITH  PJP-4  	     71

 23  COMPARISON OF DEGRADATION RATES IN THE ESCAMBIA RIVER  TEST  	     73

 24  RATE OF DISAPPEARANCE OF SELECTED SJP-4 HYDROCARBONS  IN  RANGE

     POINT TEST 	     82

 25  RATE OF DISAPPEARANCE OF SELECTED PJP-4 HYDROCARBONS  IN  RANGE

     POINT TEST 	     83

 26  COMPARISON OF BIOTIC DEGRADATION RATES IN RANGE POINT  TEST  	     84

 27  COMPARISON OF ABIOTIC DEGRADATION RATES IN RANGE POINT TEST 	    86
                                       IX
                      (The reverse of this page is blank.

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                                Section I





                               INTRODUCTION





A.  OBJECTIVE



    The Air Force uses large quantities of hydrocarbon fuels and is



currently evaluating the fuels derived from shale oil.  The use of these



fuels introduces the possibility of their accidental release into the



environnment and requires that their fate and effects in the environment,



be understood.  The information available on shale derived jet fuel  is



insufficiently detailed to permit predictions about the extent and



importance of biological degradation in aquatic ecosystems.  Therefore,



the purpose of this project was to characterize, in laboratory systems,



the environmental fate of shale-derived jet fuels.  Specific objectives



were to:



    a.  Develop the necessary analytical procedures to chemically



        characterize the shale-derived jet fuel.



    b.  Compare the chemical composition of shale-derived jet fuel



        with petroleum-derived jet fuel.



    c.  Examine the biotic and abiotic fate of shale-derived jet



        fuel and compare results with previous studies on petroleum-



        derived jet fuel.



    d.  Characterize some of the factors affecting the biotic and



        abiotic fate of shale-derived jet fuel.



B.  BACKGROUND



    Physical characteristics of shale-derived JP-4 are similar to those



of the petroleum-derived product.  This is to be expected as these



characteristics are reflections of the suitability of shale oil  products





                                    1

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as a replacement for petroleum-derived JP-4.  Several  of these physical



characteristics, as reported by Ghasseml _et_ ji]_.  (Reference 1), are



summarized In Table 1.



     Gas chromatographlc characterization of fuel oil  hydrocarbons pro-



vides a means of assessing their compositions.  Examination of 33 indivi-



dual hydrocarbons common to the petroleum- and shale-derived fuel oils,



as reported by Hayes and Pitzer (Reference 2), shows some of the simi-



larities in the oils.  A comparison of the fuels is shown in Table 2.



     The n-alkanes comprise about 54 percent of the analyzed hydrocarbons



in the petroleum-derived JP-4 and about 68 percent in the shale-derived



JP-4.



     Branched chain hydrocarbons were generally higher in the petroleum-



derived fuel; they were 3 and 5 times greater for the mono- and di-substi-



tuted alkanes, respectively.  The known slow biodegradation of branched



alkanes relative to straight chain alkanes suggests that petroleum-derived



fuels would persist longer in aquatic environments.



     The other hydrocarbon groups comprise a much smaller percentage of



the total fuel.  Variability in the analysis of these minor hydrocarbons



does not allow generalizations to be made, except that compositional



differences are  small.



     Hayes and Pitzer (Reference 2) published gas chromatographic results



(area percent) of an extensive analysis of both petroleum-based and shale-



derived JP-4.  They found wide compositional differences in the same fuel



type, depending  on when samples were taken during the various handling pro-



cesses.  High volatility of many of the fuel hydrocarbons makes detailed



comparisons of jet fuel samples difficult.

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             TABLE 1.   PHYSICAL CHARACTERISTICS  OF  JET  FUELa
                                                  SHALE
                                                  JP-4

                                                   52.3

                                                     -81

                                                    2.3

                                                  18,590

                                                    0.001
PARAMETER
API Gravity0
Freezing Point ( °F)
Vapor Pressure (PSIA)
Heating Value (BTU/lb)
Sulfur (wt %)
PETROLEUM
JP-4
53.5
-79
2.5
18,702
0.03
a Values are means:   for petroleum JP-4,  N  =  26;  for  shale  JP-4,  N =  3

  Source:  Ghassemi  (Reference 1).

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 TABLE 2.  COMPARISON OF SHALE-DERIVED JP-4 WITH PETROLEUM-DERIVED JP-4,
           LITERATURE VALUES9
Constituent
N-Aklanes
Heptane
Octane
Nonane
Decane
Indane
Undecane
Dodecane
Tridecane
Tetradecane
Pentadecane
Total
Mono-Substituted Alkanes
3-Methyl hexane
2-Methyl heptane
3-Methyl heptane
Total
Multi-Substituted Alkanes
2,3-Dlmethyl pentane
2, 5-Dlmethyl hexane
254-D1methyl hexane
Total
Cycl ohexanes
Cyclohexane
Methylcyclohexane
Ethyl cyclohexane
Percent
Shale-derived JP-4
4.73
7.48
7.24
11.25
0.42
16.62
11.49
6.07
3.19
0.96
68.68
3.05
3.08
1.64
7.77
0.18
0.63
0.81
1.52
5.68
Composition
Petroleum-derived JP-4
15.76
6.60
2.54
2.24
0.17
4.17
5.25
4.71
1.02
1.35
53.77
14.39
6.14
7.19
27.72
1.48
2.52
4.00
2.13
2.17
    Total                             7.20                      4.30

Mono-Substituted Aromatlcs

Methylbenzene                         3.77                      3.41

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 TABLE 2.  COMPARISON OF SHALE-DERIVED JP-4 WITH PETROLEUM-DERIVED JP-4,
           LITERATURE VALUES3 (CONCLUDED).
                                           Percent Composition
Constituent                     Shale-derived JP-4     Petroleum-derived JP-4

Multi-Substituted Aromatlcs

1,3,5-Trimethylbenzene                1.52                       1.09
1,2,4-Tn'methyl benzene                2.00                       3.52
1,2,3-Trimethylbenzene                0.30                       1.04

    Total                             3.82                       5.65

Xylenes

m-Xylene                              2.60                       2.71
£-Xylene                              1.70                       1.63
o-Xylene                              2.00                       1.89

    Total                             6.30                       6.23


Note:  Totals do not necessarily equal 100 percent due to rounding error.

a Reference 2.

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C.  SCOPE/APPROACH



    The approach of the project was to initially develop analytical



methods to compare the chemical composition of shale-derived jet fuel



with petroleum-derived jet fuel.  Capillary gas chromatography would be



used to characterize compositional differences.  Differences in the hydro-



carbon composition of the water soluble fraction would be compared using



standard techniques (Reference 3)  and chromatographic analysis of solvent



extracts.



    Second, the quiescent bottle test, developed for previous JP-4 studies



(Reference 4) would be used to assess the biotic and abiotic fate of shale-



derived jet fuel in water and  sediment samples taken from three estuarine



sites.  Conditions for optimizing the quiescent bottle test would also



be established.  Biodegradation would be verified with mineralization



studies.  Relationships between volatility in these tests and volatility



in a system designed to model  a jet fuel  spill would be further examined.



    Third, environmental conditions which might affect the biotic and



abiotic fate of jet fuel would be tested.  Factors such as dissolved organic



carbon and toxicity to microbial communities would be investigated.

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                                Section II

                                 METHODS



A.  JET FUEL

    The jet fuel  (SJP-4)  supplied by the Air Force for our studies

was received in a 55-gallon metal drum labeled with the following

information.

                                     F-40
                                     JP-4
                            Turbine Fuel Aviation
                                 MIL-T-5624L
                            NSN 91300-00-256-8617
                        (Refined From Shale Crude Oil)
                                 Batch No. 1
                              Geokinetics, Inc.
                               Caribou Refinery
                          Woodcross, Utah 84087
                         Inital boiling pt. 130°F
                          Flash pt. below -20°F.


    Subsamples of this SJP-4 and petroleum-derived jet fuel  (PJP-4)  were

diluted to a working concentration with methylene chloride (pesticide

grade), and stored in amber glass bottles with Teflon®-lined screw caps.

B.  INSTRUMENT CONDITIONS

    All hydrocarbon samples were analyzed using the following instrument

conditions:

    Instrument:  Hewlett/Packard 5730A gas chromatograph
    Column:  Capillary, approximately 60 m x 0.25 mm
    Coating:  SPB-1
    Injector:   Hewlett/Packard 7671A, 1 u£ injection volume
    Data Handling:  Hewlett/Packard 3357 Lab Automation System
    Plotter:  Hewlett/Packard 3380A integrator
    Detector:   Flame lonization at 250°C
    Injection:   Split/splitless, splitless mode at 250°C
    Oven Temperatures:
         Initial:   20°C (cyrogenic)  for 2 minutes
         Rate:   2°C per minute
         Final:  190°C  for  8 minutes

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 C.   METHOD  REFINEMENTS



     1.   Extraction  Procedure



         Preliminary  investigations conducted  in preparation for full scale



rate  testing with shale oil-derived JP-4 jet  fuel gave rise to several



 questions regarding  the efficacy of the extraction procedures used  on



 sediment/water  slurries in  previous tests.



         In  the  past, sediment/water slurries  were treated as a discrete



 sample;  they were decanted  from the test bottle into a separatory funnel



 and  extracted with methylene chloride.  Spike recovery tests done prior



 to previous tests indicated that the method gave good analytical results



 if extraction times  were  1  hour or greater.   The results of prototype



 tests with  SJP-4, however,  indicated that increased contact time between



 the  fuel and the sediment may have a significant negative impact upon the



 ability  of  methylene chloride to remove hydrocarbons from the sediment.



 Additionally, Lake _e_t jil_. (Reference 5) indicated that they found methy-



 lene  chloride to be  less  than ideal as an extracting solvent for sediment/



 soil  systems.



         An  alternative for  analyzing sediment/water slurries in the SJP-4



 biodegradation  studies was  to fractionate the sample by centrifugation of



 the  sediment, decant the  water, then treat the two samples separately.



 This  procedure  will  be referred to as the fractionated sample method.



 Although several solvents have been used for sediment extractions,  aceton-



 itrile is probably the most commonly used.   Acetonitrile was tested as



 the  sediment-extracting solvent in this analytical  method.   Methylene



 chloride was retained as  the extracting solvent for the water fraction of



 these samples.

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        To compare the two analytical methods (discrete versus fraction-
ated), a standard quiescent bottle test (all nonsterile systems) was set
up, using two sediment concentrations;  500 and 5,000 mg/t, each in
duplicate.  Bottles containing 25 m£ of water were spiked with 250 M£ of
SJP-4, shaken for  l  hour on a shaker table, then placed on their sides
on a lab bench for 24 hours with the bottle caps removed.  Following 24
hours of incubation, the contents were extracted, using the fractionated
and discrete sample methods described above.  Extracts were analyzed by
gas chromatography.
        The results of the method test (Figures 1 and 2)  indicated that
the new fractionation method was more effective in recovering hydrocarbons
that have been in contact with sediment.  The new method resulted in
recoveries of 93 percent of the original spike whereas the previous dis-
crete method resulted in maximum recoveries below 60 percent of the
original SJP-4 spike.
        The amount of fuel recovered from the water was about the same
(55-60 percent)  as that recovered from the total sample by the discrete
method.  This suggests that the methylene chloride was leaving much of
the hydrocarbons on the sediment after a short extraction.  Therefore,all
subsequent test samples requiring extraction were analyzed using the
fractionation method.
    2.  Quiescent Bottle Test
        Our primary test system consisted of the standard quiescent bottle
test as described by Spain ^t aj_. (Reference 4).  The test system used
150 ms, milk dilution bottles with Teflon®-lined plastic screw caps.  Each
bottle contained 25 ml of water or sediment/water slurry from the test site
in question.   At test initation each bottle was spiked with 250 yf, of jet

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   3000


   2500
TOTAL
OIL 2000

CONC
    1500


    1000


    500


      0
MG/L
                METHYLENE  CHLORIDE/
                ACETONITRILE EXTRACTIONS
                METHYLENE
                 CHLORIDE
                                           ACETO-
                                           NITRILE
             102%
                         500 MG/L SEDIMENT
                                           44%
            SEPARATE
                                                COMBINED
                         EXTRACTION
                            MODE
  Figure 1.  Extraction Methodology with 500 mg/£ Sediment
                       10

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   3000
   2500

TOTAL
OIL 2000
CONG

   1500
    1000


    500


      0
       MG/L
                       METHYLENE CHLORIDE/
                       ACETONiTRILE EXTRACTIONS
                       METHYLENE
                        CHLORIDE
                       ACETO-
                       NITRILE
94%
                                5000 MG/L SEDIMENT
                              60%
                   SEPARATE
                            COMBINED
                                EXTRACTION
                                   MODE
         Figure 2.  Extraction Methodology with 5,000 mg/x.  Sediment
                              11

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fuel, Immediately capped, then shaken for 1 hour.  The bottles were then



uncapped and placed on their sides on a 1 ab bench.  Sterile controls were



similar to nonsterile bottles except for the addition of formalin to a



final concentration of 2 percent.  Duplicate bottles of each sample type



(water, sediment/water slurry; active and  sterile)  were sacrificed at



each sampling interval, analyzed as described above and the duplicate



results averaged.



    Where the effect of sediment concentration was tested,  500,  1000,



2000, and 5000 milligrams of sediment per  liter of water were used.



Bottles were spiked with 200 y£ of SJP-4,  shaken for 1 hour, then incu-



bated with the tops removed.  Bottles were sacrificed at 0, 24,  48, and



96 hours.  The sediment and water in each  bottle were analyzed separately



for hydrocarbon content using methods described above.



D.  SAMPLING SITES



    Sediment and water were collected from three test sites:  Range Point



salt marsh, located on Santa Rosa Island;  Bayou Chico, a brackish extension



of Escambia Bay; and Escambia River, a freshwater river adjacent to



Pensacola.   Range Point salt marsh and Escambia River are considered to



be relatively pristine having little or no input from industrial or



municipal  effluent.  Bayou Chico, however, is heavily polluted.



E.  COMPOSITIONAL ANALYSIS



    1.   Neat Fuel



        Composition of shale-derived jet fuel  was determined by two methods,



First,  a sample of the SJP-4 and the PJP-4 were diluted to working con-



centration  (3 y£/m£)  with methylene chloride and analyzed by gas chromato-



graphy.   Concentrations of 32 selected hydrocarbons (Table 3) in each jet



fuel  sample were then compared to each other as well as to values for the





                                    12

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same hydrocarbons as reported by Hayes and Pitzer (Reference 2) .



    Second, the samples of SJP-4 and PJP-4 were fractionated by silica gel



chromatography into aromatic and aliphatic components.  One m£  samples of



each fuel (SJP-4 and PJP-4) were added to the top of 25 cm by 1 cm silica



gel columns which were filled with petroleum ether.  Aliphatics were



eluted with two 25 m£ washes of petroleum ether.  Aromatics were eluted



with two 25 mst washes of methylene chloride.  The combined eluates were



then subjected to gas chromatographic analysis and comparisons made by



summing the total area of  all peaks found in each fraction.



2.  Water-Soluble Fraction



    Experiments were conducted to establish the reproducibility of the



water-soluble fractions (WSF) generated from both PJP-4 and SJP-4 The



method of Hunt (Reference  3) was used to obtain the water soluble fract-



ions.  Each WSF was made in a 4-liter aspirator bottle with a tube con-



nector at the bottom of the bottle.  Two liters of filtered seawater



(0.45 micron  filtration) were placed in each bottle and 200 milliliters



of the JP-4 were gently spread across the surface.  The oil/water system



was then stirred overnight with a Teflon®-coated magnetic stirring bar



such that the oil vortex extended down one-third of the water depth.  To



circumvent any possible loss due to volatilization the oil content of the



system was increased from  5 to 10 percent of the water volume.  Hunt's



investigation indicated that this would have no effect on the hydrocarbon



content of the WSF.



    The system was allowed to settle for 1 hour after stirring.  A 1-liter



water sample was then removed from the bottom of the bottle through the



tube connection, extracted twice with methylene chloride, and the combined



extracts  were analyzed for hydrocarbon content.





                                    13

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   TABLE 3.  LIST OF COMPONENT HYDROCARBON MONITORED THROUGHOUT STUDIES
BENZENE




CYCLOHEXANE




2,3-DIMETHYLPENTANE




3-METHYLHEXANE




HEPTANE




METHYLCYCLOHEXANE




2,5-DIMETHYLHEXANE




2,4-DIMETHYLHEXANE




METHYLBENZENE (TOLUENE)




2-METHYLHEPTANE




3-METHYLHEPTANE




1,1-DIMETHYLCYCLOHEXANE




OCTANE




ETHYLCYCLOHEXANE




ETHYLBENZENE




m-XYLENE
£-XYLENE



^-XYLENE



NONANE



ISOPROPYLBENZENE (CUMENE)



1,3,5-TRIMETHYLBENZENE



1,2,4-TRIMETHYLBENZENE




DECANE



1,2,3-TRIMETHYLBENZENE




INDAN



UNDECANE



NAPHTHALENE



DODECANE



TRIDECANE



TETRADECANE



PENTADECANE



HEXADECANE
                                    14

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F.  TOXICITY TESTS



    Toxicity to the natural microbial community was investigated by assess-



ing the ability of the natural microflora to mineralize a test substrate



following exposure to SJP-4.



    Water from each test site was exposed to SJP-4 for 48 hours in the



standard quiescent bottle test system.  The exposed water was spiked with



20 mg/£ of ^C labeled toluene and then sealed in the milk dilution



bottles.  Controls consisted  of untreated site water, site water pre-



exposed to SJP-4 plus 2 percent formalin and site water preexposed to



unlabeled toluene.  All controls were spiked with 20 mg/£ of ^C labeled



toluene along with the water  preexposed to SJP-4.



    Following 24 hours of incubation, the contents of each sealed milk di-



lution bottle were acidified  by injection of IN HC1 .  The acidified



solution was bubbled with nitrogen to purge C02 into traps containing IN



NaOH.  1^002 was quantitated  in subsamples of NaOH by liquid scintillation
counting.  The water in the bottle was then subsampled for residual



G.  DISSOLVED ORGANIC CARBON



    The effect of dissolved organic carbon (DOC) on hydrocarbon solubility



was investigated using a fulvic acid solution prepared from digested Range



Point detrital sediment by the procedure of Boehm and Quinn (Reference 6) .



The thick detrital sediment slurry was adjusted to a pH of 9 with NaOH and



allowed to stand 24 hours.  The slurry was then acidified with HC1 to a pH



of 1 and again allowed to stand 24 hours, and the resulting solution was



adjusted to pH 7 with NaOH, then filtered through glass fiber filters to



remove any undigested material.  This solution was used to amend water



collected from Range Point.  DOC concentrations of the unamended water and



the fulvic acid stock solution were measured before testing with a total





                                    15

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organic carbon analyzer.  Initial DOC of the unamended seawater was 20 mg/A



and the fulvic acid stock solution was 400 mg/m£ .



H.  JET FUEL EVAPORATION RATES



    Simple experiments were conducted to estimate evaporative loss of SJP-4



in the absence of confusing factors such as solubilization of jet fuel com-



ponents into the water.  The test system consisted of glass petri dishes



(10 cm diameter by 1 cm deep)  filled with 60 m£  of SJP-4.  Five dishes were



set up in a fume hood with a measured air flow of 50 cubic feet/minute.  Con



tents of dishes were weighed at intervals and an evaporative loss percent



was obtained by weight difference.
                                    16

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                               Section III






                                 RESULTS





A.  COMPOSITIONAL ANALYSIS



    1.  Fuel



        Table 4 compares the concentration (percent of total) of 32 selected



hydrocarbons in each of the jet fuels with the same 32 hydrocarbons found in



shale- and  petroleum-derived jet fuels studied by Hayes and Pitzer (Reference



2; Table 2).  Compositional differences betweeen the jet fuels were generally



small.   N-alkanes accounted for over 50 percent of the total hydrocarbons in



all fuels.  Aromatics accounted for an average of 12 percent; substituted



n-alkanes and cycloalkanes made up the remainder of the fuels.



        Results of the analysis of the fuels following silica gel fraction-



ation are presented in Figure 3.  There was little apparent difference between



the two fuels; SJP-4 consisted of 67 percent aliphatics and 33 percent aro-



matics and  PJP-4 consisted of 60 percent aliphatics and 40 percent aromatics.



As the analysis was only accurate to ± 9 percent, differences were considered



insignificant.



    2.  Water Soluble Fraction



        The hydrocarbon compositions of the WSF from each fuel were very simi-



lar both within replicates and between experiments (Table 5).  Total  hydrocar-



bon concentrations in the WSF were similar to those found by Hunt (Reference



3).  Mean hydrocarbon concentration in our experiments were 101 mg/£  and 84



mg/£  for petroleum- and shale-derived JP-4, respectively; Hunt reported a



maximum concentration of 45 mg/a  with the JP-4 used in his experiments.



        The major compositional  difference in the WSF of PJP-4 and SJP-4 was



the concentration of benzene.  Benzene concentrations were 44 mg/£  and



                                    17

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  TABLE  4.   COMPARISON OF  SHALE-DERIVED  JP-4  WITH  PETROLEUM-DERIVED JP-4,
            ACTUAL  VALUES
Constituent
N-Alkanes
Heptane
Octane
Nonane
Decane
Indane
Undecane
Dodecane
Tridecane
Tetradecane
Pentadecane
Total
Mono-Substituted Alkanes
3-Methylhexane
2-Methyl heptane
3-Methyl heptane
Total
Multi-Substituted Alkanes
2,3-Dimethyl pentane
2,5-Dimethylhexane
2,4-Dimethylhexane
Total
Cyclohexanes
Cyclohexane
Methyl cyclohexane
Ethyl cyclohexane
Percent
Shale-derived JP-4
2.61
2.99
4.93
6.26
1.00
8.19
10.08
9.35
4.80
1.86
52.07
4.37
1.10
4.22
9.69
1.24
1.13
1.32
3.69
0.97
5.88
3.96
Composition
Petroleum-derived JP-4
7.62
9.94
6.31
5 65
0.48
6.53
7.32
5.77
3.25
1.01
53.88
3.94
5.30
5.71
14.95
1.08
0.82
1.76
3.16
2.20
0.48
2.79
     Total                        10.81                          5.47

Mono-Substituted Aromatlcs

Methyl benzene                      5.40                          3.27
                                    18

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 TABLE 4.  COMPARISON OF SHALE-DERIVED JP-4 WITH PETROLEUM-DERIVED JP-4,
           ACTUAL VALUES (CONCLUDED)
 Constituent

Multi-Substituted Aromatlcs

1,3,5-Trimethyl benzene
1,2,4-Trimethyl benzene
1,2,3-Trlmethyl benzene

     Total

Xylenes

m-Xylene
£-Xylene
£-Xylene

    Total
            Percent Composition

Shale-derived JP-4        Petroleum-derived JP-4
    3.12
    1.41
    0.60

    5.13
    3.61
    2.35
    3.36

    9.32
2.17
0.52
1.48

4.17
2.57
1.88
1.72

6.17
Note:  Totals do not necessarily equal 100 percent due to rounding error.

Based on percentage area of gas chromatographic peaks for the selected
32 hydrocarbons only.  Values based on the mean of duplicate samples.
Maximum analytical error for any single hydrocarbon was never greater
than ±9 percent.
                                    19

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             S-JP4
                                 P-JP4
Aromatics
Aliphatics
Aromatics
Aliphatics
               Figure  3.   Silica Gel  Fraction
                              20

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                TABLE  5.   WATER  SOLUBLE-FRACTION COMPONENTS
Constituent
Benzene
Cyclohexane
3-Methylhexane
Heptane
Methylcyclohexane
Methyl benzene
Ethylbenzene
nv-Xylene
jp_-Xylene
j3-Xylene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,3-Trimethylbenzene
Indan
n-Undecane
Naphthalene
n-Tridecane
  Mean Hydrocarbon Level s ui_ WSF, Mean jcrf
4 Replicates,mg/£ (±/- 1 Standard Deviation)
                                   Petroleum
                                      JP-4
    44.2 (0.53)
     2.7 (0.15)
    13.8 (0.35)
     1.6 (0.35)a
     1.0 (0.05)
    27.8 (1.19)
     2.2 (0.10)
     5.4 (0.14)3
     3.8 (2.40)
     3.5 (0.15)b
     0.5 (0)b
     1.9 (0.29)
     0.9 (0.08)
     0.3 (0)
     1.1 (0.12)
     0.2 (0.06)
                              Shale Oil
                                JP-4
19.2  (0.89)
 0.7  (0.05)
13.2  (0.95)
 0.8  (0.05)
33.0  (1.63)
 1.7  (0.08)
 5.6  (0.22)
 2.0  (0.06)
 4.4  (0.17)
 0.5  (0.14)
 1.7  (0.10)
 0.4  (0)
 0.4  (0.05)
 0.3  (0)
Total   Hydrocarbons             101.2  (7.45)
aMean and standard deviation of  2  replicates.
&Mean and standard deviation of  3  replicates.
      Not Detected
                             84.2   (3.90)
                                     21

-------
 19  mgA,  respectively.  This difference accounted for the difference in



 mean  total  hydrocarbon concentrations.



 B.  BOTTLE  TEST OPTIMIZATION



    As  a  preliminary test in preparation for quiescent bottle tests with



 SJP-4 we  determined the optimal sediment concentration to be used in the



 bottle  test.   Previous observations that sediment concentrations might



 have  a  significant impact on test results, required that we delineate the



 role  of sediment concentration in the quiescent bottle test.



    The results of the tests (Figure 4)  indicated little effect of sediment



 concentrations after the first 24 hours.  Although the total recovery seemed



 to  be affected at 24 hours, ranging from 28 percent in the 500 mg/£ bottle



 to  58 percent  in the 2000 mgA bottle, by 96 hours, all  results were nearly



 identical,  with total recoveries of about 24 percent and a partitioning of



 about 22  percent of that total onto the sediment.



 C.  QUIESCENT BOTTLE TESTS



    1.  Range  Point



        A large decrease in total  hydrocarbon concentration during the first



 four  hours  of  incubation occurred in all treatments (Figure 5).  Volatilization



 played a major role in hydrocarbon disappearance, as evidenced by the losses



 from  sterile systems.  As expected, this volatility had a greater impact upon



 lower boiling hydrocarbons.  Major differences were also seen between sterile



 and active  water systems, indicating biodegradation (Table  5A).  The presence



 of sediments generally reduced volatility in sterile systems and effectively



 eliminated biodegradation in most of the water systems.  We currently have no



explanation for this effect of sediments on biodegradation.



        Similar results  were observed in previous tests with petroleum-derived



JP-4 (Reference 4),  although loss of hydrocarbons in their nonsterile water






                                    22

-------
                                  "=0
                    WATER
      MG/L
  2000
0
I
   1500
C
0  1000
N
C
   500
 SEDIMENT
 ESSSS
TOTAL
                           1000            2000
                         SEDIMENT CONCENTRATION
                                 (MG/U
                        5000
                                1=24
                   WATER
SEDIMENT
TOTAL
    MG/L
                         1000            2000
                       SEDIMENT CONCENTRATION
                                (MG/L)

   Figure  4.  Effect  of Sediment  Concentration
                        5000
                          23

-------
    100 r—
cu   80
"a.
CO
 ^_
O

"o
-t-j
c:
CD
o
i. —
a>
Q_
+ STERILE SEDIMENT

* STERILE WATER

H NONSTERILE SEDIMENT

x NONSTERILE WATER
                                                            20
      Figure 5.  Total Hydrocarbon Loss in Range Point Bottle Test
                            24

-------
    TABLE 5a.  COMPARISON OF DISAPPEARANCE RATES IN STERILE AND ACTIVE
               RANGE POINT SYSTEMS
Slope of semi -log
Hydrocarbon
2,3-dimethylpentane
3-Methylhexane
Heptane
Methyl cycl ohexane
2,5-Dimethylhexane
2,4-Dimethylhexane
Methyl benzene
2-Methyl heptane
3-Methyl heptane
Octane
Ethyl cycl ohexane
Ethyl benzene
ni-Xylene
£-Xylene
£-Xylene
Nonane
Isopropyl benzene
plot concentration
Sterile9
-.0028
-.0038
-.0030
-.0138
-.0016
-.0017
-.0769
-.0014
-.0015
-.0012
-.0012
-.0018
-.0359
-.0014
-.0020
-.0007
-.0007
(mg/£) versus
Active
-.0496
-.0713
-.0899
-.0775
-.0513
-.0540
-.0746
-.0742
-.0720
-.0679
-.0728
-.0562
-.0691
-.0610
-.0689
-.0709
-.0060
time
Ratio of Active
to Sterile Rates
17.7
18.8
30.0
5.6
32.1
31.8
-0.97
53.0
48.0
56.6
60.7
31.2
1.9
43.6
34.4
101.3
8.6
  Disappearance of hydrocarbons from shale-derived JP-4 in quiescent
  bottle tests containing water from Range Point salt marsh

aSterilized by addition of formalin to the water to a final  concentration
 of 2%.
                                    25

-------
systems was less extensive than observed in this test.   Figures  6 through
16 present the relative loss rates of the 32 individual  hydrocarbons
monitored throughout the test.
        Comparison of our results with those reported for  previous  PJP-4
tests (Reference 4) indicated a significant difference  in  the  disappearance
rates of many of the hydrocarbons.  The faster  disappearance of  the hydro-
carbons in the PJP-4 test was due to a greater  volatility  of the hydro-
carbons in that test (as evidenced by disappearance  rates  in the sterile
systems).  The SJP-4 data indicated an approximate 5 to  10-fold  increase
in rate between sterile and nonsterile water for compounds such  as  decane,
undecane and naphthalene; the results of the PJP-4 test  indicate approxi-
mately two-fold differences.  Additionally, 95  percent  confidence limits
for the rates indicate that in some cases (decane, for  example)  the
difference between sterile and nonsterile water systems  was significant
in the SJP-4 test (confidence limits do not overlap) but not significant
in the PJP-4 test (confidence limits do overlap), although disappearance
rate in the nonsterile PJP-4 test is over twice as fast  as the corresponding
rate in the SJP-4 test.  This lack of difference in  the  PJP-4  test  is
likely due to the sampling schedule, i.e., the  initial  drop in (decane)
concentration within the first 24 hours was such a heavily weighted
portion of the disappearance curve, that any later biodegradation was
below detection limits.
        The differences between sampling schedules,  possible differences
in test conditions and probable environmental changes  at the test site
make comparison of the SJP-4 data with any previous  tests  difficult.
        Mineralization of 14C decane showed that approximately 60,000 dpm
of 14C02 (7 percent of the original spike) were produced in the  nonsterile

                                    26

-------
       80—1
C
0
N
C

M
5
      68 —
40-:
                                ETHYLCYCLOHEXANE
                                              Sterile  Water  	*
                                              Active Water  -.-.A
                                              Sterile  Sediment  ....X
                                              Active Sediment       o
                                   DAYS
C
O
N
C

M
5
                                 BENZENE
                                              Sterile Water	*
                                              Active Water -.-.A
                                              Sterile Sediment ....X
                                              Active Sediment       o
        2 —
                T[II"TII[[II[I[TtIII
                         E             10             is            ze>
                                   DAYS
       Figure  6.   Loss  of  Ethylcyclohexane  and  Benzene in  Range Point Test
                                        27

-------
c
0
N
C

M
S
          -4
                                CYCLOHEXANE
                                    r-p-r
                                      ta
                                   DAYS
Sterile Water	*
Active Water -.-.A
Sterile Sediment ....X
Active Sediment 	o
IS
I   i   1  i  I
          20
C
0
N
C
/
L
                                METHYLCYCLOHEXANE
Sterile Water 	*
Active Water -.-.A
Sterile Sediment  ....X
Active Sediment       o
                                   DAYS
      Figure 7.  Loss of Cyclohexane and Methylcyclohexane in Range Point Test


                                       28

-------
       aa—i
c
0
N
C

M
6
40 —
       20-
        a-
                                METHYLBENZENE
                                             Sterile Water 	*
                                             Active Water -.-.A
                                             Sterile Sediment ....X
                                             Active Sediment       o
c
— v~ T— T— r — | — r — r ~
i E
i i | i i i
10
1 1 '
IE
1 1 1 |
20
                                   DAYS
c
0
N
C

M
G
          a
                                ETHYLBENZENE
                                             Sterile Water ---- *
                                             Active Water -.-.A
                                             Sterile Sediment
                                             Active Sediment
                                                                         X
     Figure 8.  Loss of Methylbenzene and Ethylbenzene in Range Point Test
                                       29

-------

c
0
N
C
M
S
/
L


3 —
2 —
H
•4
1 . 1
I ' •
-
ra __
ISOPROPYLBENZENE
\ Sterile Water 	 *
\ * Active Water -.-.A
[\ /\ Sterile Sediment ....X
\ */ \ Art.ive Sediment o
•W
W t.::.::.-,.. 	 =<•,
\ x / — —•*•-.>-,..__ 	
. vw-v. X •*
\ \7X
t i / \ »«
\ \t \
i tf , X. 	 ..._^j^- — ,
          a
        T—r—9—r
                   ia            IE
                DAYS
C
O
N
C

M
G
                                 m-XYLENE
                                  Sterile Water 	*
                                  Active Water -.-.A
                                  Sterile Sediment ....X
                                  Active Sediment       o
f~¥ — [ — i — t — i — i — [ — i — i — i — i — [ — i — i
      E             IB             IE
                DAYS
                                                                  20
        Figure 9.  Loss of Isopropylbenze and ni-Xylene in Range Point Test
                                        30

-------
c
o
N
C

M
6
C
O
N
C

M
G
                                p-XYLENE
Sterile Water 	*
Active Water -.-.A
Sterile Sediment ....X
Active Sediment       o
                                   DAYS
                                o-XYLENE
Sterile Water 	*
Active Water -.-.A
Sterile Sediment  ....X
Active Sediment       o
        0
                                   DAYS
         Figure 10.  Loss of £-Xylene and £-Xylene  in Range  Point  Test
                                        31

-------
       63—r
C
o
N
C

M
G
C
O
N
C

M
                             1,3,5-TRIMETHYLBENZENE
 Sterile Water 	*
 Active Water -.-.A
 Sterile Sediment  ....X
 Active Sediment 	o
                                        T—i—r
~r
 IE
                                                      T—i—r
-'"I
  20
                                   DAYS
       ea
                             1,2.4-TRIMETHYLBENZENE
 Sterile  Water  	*
 Active Water  -.-.A
 Sterile  Sediment  ....X
 Active Sediment       o
      za—

(
V.
— i — i—*r
»

-tit*
E

—i — r-

10

J 1 "'T-

IS 2
                                  DAYS
      Figure 11.  Loss of 1,3,5-Trimethylbenzene and 1,2,4-TMmethylbenzene
                  in Range Point Test
                                       32

-------
c
0
N
C

M
s
        a
                            1,2,3-TRIMETHYLBENZENE
Sterile Water 	*
Active Water -.-.a
Sterile Sediment ...
Active Sediment
VN
! """"-A.
| 1 1 I T
a

^-^—
\ ' '
E

. a B""
I I | 1 1 1
ia
PAYS
	
1 I '
IE

— *
I 1 > 1 |
2B

c
o
H
C

M
C
                             INDAN
Sterile Water 	*
Active Water -.-.A
Sterile Sediment  	X
Active Sediment       o
          a
                                   PAYS
   Figure  12.   Loss  of 1,2,3-Trimethylbenzene and Indan and Range Point Test
                                       33

-------
      200
C
o
N
C

M
G
      ice—
tea
       sa—
                             HEPTANE
                                              Sterile Water 	*
                                              Active Water -.-.A
                                              Sterile Sediment ....X
                                              Active Sediment       o
       SB—i
c
o
N
C

M
C
                             OCTANE
                                              Sterile Water 	*
                                              Active Water -.-.A
                                              Sterile Sediment  ... .X
                                              Active Sediment       o
                                   PAYS
            Figure  13.   Loss  of  Heptane  and  Octane  in  Range  Point  Test
                                        34

-------
                            NAPHTHALENE
C
0
N
C

M
S
                                                   Sterile Water 	*
                                                   Active Water -.-.A
                                                   Sterile Sediment ....X
                                                   Active Sediment       o
       a
                                  DAYS
          Figure 14.  Loss of Napthalene in Range Point Test
                                       35

-------
      80—i
                             NONANE
c
0
N
C
       a
          3
                                                    Sterile Water	*
                                                    Active Water -.-.A
                                                    Sterile Sediment  ....X
                                                    Active Sediment 	o
C
o
N
C

M
S
                              DECANE
                                                    Sterile Water 	*
                                                    Active Water -.-.A
                                                    Sterile Sediment ....X
                                                    Active Sediment       o

       0

          3
                                     18

                                  DAYS
T—p-r~Tr*r"t—j
   16            20
            Figure 15.   Loss of Nonane and  Decane  In  Range Point Test
                                        36

-------
C
0
N
C

M
6
                            PENTADECANE
Sterile Water 	*
Active Water -.-.A
Sterile Sediment ... .X
Active Sediment 	o
          	x
c
o
N
C
M
C
/
u
z.a-^
«
M
l.E —
*•
*•
1 .a—
M
0.S— '

.8
C
HEXADECANE
ft Sterile Water 	 *
A Active Water -.-.A
I \ Sterile Sediment ....X
1 • Active Sediment o
/ \
*' \
/« ^
/K >,.
uJ V \ 	 ^.-^..^^
**»j^»»-*^t^^^ * * ~-~ )ic-_rr^ 	 o
iiiiiiiiiiiiiiiiiitt
i c ia ic 20
                                   PAYS
       Figure 16.  Loss of Pentadecane and Hexadecane in Range Point Test
                                       37

-------
flask and only 600 dpin (< 0.01 percent of the original  spike)  were pro-



duced from the sterile flasks.  This confirms that  partial  disappearance



of decane in the bottle test was the result of biodegradation.



    2.  Bayou Chico



        The Range Point test clearly demonstrated difficulties  in  trying



to compare results of current SJP-4 test with previous  PJP-4 tests,  con-



sequently the quiescent bottle test system was expanded to  include both



SJP-4 and PJP-4.  The results are shown in Tables 6 -  13.



        Volatilization played a predominant role  in hydrocarbon  disappear-



ance for this test.  Unlike previous tests, however, the volatility



virtually overwhelmed our ability to detect biodegradation  as evidenced



by the lack of statistically significant differences in the disappearance



rate between nonsterile and sterile systems (Table  14).  Comparison  of



results with the two types of jet fuel, SJP-4 and PJP-4, show that there



was no significant difference in disappearance rates although,  as  one



would expect when volatility plays such a predominant  role, the lower



boiling hydrocarbons are lost faster than the higher boiling hydrocarbons.



        Subsequent investigations with radiolabeled decane  and 2-methyl-



naphthalene showed that, despite the lack of apparent  biodegradation based



on the disappearance of parent compound, some biodegradation (mineralization



to C02)  was occurring.



    3.  Escambia River



        Data from the quiescent bottle test with  both  SJP-4 and PJP-4 and



water/sediment samples from Escambia River are presented in Tables 15 - 22.



Volatilization was again the predominant factor in  hydrocarbon removal.



Disappearance patterns of the individual hydrocarbons  were  similar to those



seen in previous tests, i.e., lower boiling hydrocarbons were lost faster






                                    38

-------
                               TABLE  6.   DATA FROM BAYOU CHICO BOTTLE TEST, STERILE  WATER  WITH SJP-4
OJ
Hydrocarbon



Benzene



Cyclohexane



2,3-dimethylpentane



3-Methylhexane



Heptane



Methylcyclohexane



2,5-Dimethylhexane



2,4-Dlmethyl hexane



Methyl benzene



2-Methylheptane



3-Methylheptane
 Day 0         Day 1



  9.7 (4- .3)



 14.0 (+_ .7)



 94.5 (+_  0)



 57.2 (+1.1)



175.8 (+11.4)  72.4b



 83.1 (+_ .7)



 20.7 (+_ 0)



 23.6^




 73.4 (+_ .4)



 72.6 (+_2.4)



 64.6 (+ .2)
               1,1-Dimethylcyclohexane 0.7 (+_  0)
               Octane



               Ethylcyclohexane



               Ethyl benzene



               jn-Xylene



               2-Xylene



               o-Xylene
                        52.1 (+_ .1)



                        68.5 (_+ .2)



                        27.6 (+_ .2)



                        58.2 (jf .3)



                        37.0 (+_ .1)



                        57.8 (+ .3)
                                                                 Day 2
Day 4
Day 8
Day 13
                                                                               28.4  (+  0)   45.8 (^3.6)
                 1.0  (+_ .1)



                 7.8  (+ .1)
                            4.0
  3.7  (+  .6)    2.8 (+ .5)    2.3 ( +1.7)

-------
                          TABLE 6.  DATA  FROM  BAYOU CHICO BOTTLE TEST, STEILE WATER WITH SHP-4  (CONCLUDED)


               Hydrocarbon            Day 0          Day 1        Day 2        Day 4        Day 8         Day  13

               Nonane                 33.5 (_+  .6)    10.2 (+_ .3)

               Isopropylbenzene        0.8 (_+_   0)      -

               1,3,5-Trimethylbenzene 57.7 (+_   0)    13.5 (+_ .3)    1.8 (+_ .6)    -

               1,2,4-Trlmethylbenzene 19.5 (+_  .4)     1.2 (+_ .4)    2.9 (+_ .9)    -

               Decane                119.0 (+_  .7)    51.0 (j+ .5)   15.7 (^2.6)

               1,2,3-Trimethylbenzene 11.5 (+_  .1)     4.3 (+_ .1)    1.0 (+_ .2)    -

               Indan                  22.0 (+_  .1)     6.1 (+_ .1)    2.2 (+_ .4)    -

^              Undecane               53.0 (+1.3)    11.2 (+ .5)   63.2 (+1.7)  07.9 (^19.8)
o                                           ~
               Naphthalene            10.4 (_+  .1)     7.7 (+; .1)   13.9 (^1.1)   5.4 (+_!.!)

               Dodecane               61.5 (+.1.4)     6.3 (+_ .5)  106.3 (+5.5)  26.8 (+_36.7)   9.3 (+_ .9)   0.5b(+_  .3)

               Tridecane              51.1 (+1.4)     3.3 (+2.9}  105.7 (+_1.6)  38.5 (+_45.2)  37.4 (+_7.8)   3.2  (_+  .1)

               Tetradecane            39.6 (+1.7)     4.3 (+ .7)   62.4 (+_1.2)  47.5 (+4.3)   41.0 (+_8.1)   16.4  (+1.7)

               Pentadecane            18.4 (+  .8)     1.9 (+ .1)   28.0 (+1.7)  41.3 (+_  3)   23.5 (^4.5)   19.4  (+4.3)

               Hexadecane	^_	_^	-	z	I	I	

               Concentrations (mgA)a of  selected  hydrocarbons in sterile water bottles from quiescent  bottle test,
               using water samples from Bayou  Chico and shale-derived JP-4.

               aAverage of replicate samples.
               bBad replicate; n=l
               *Parentheses indicate one  standard  deviation from the mean.
               **Dashes (-)  indicate not  detectable (<0.2 mg/n) .

-------
                  TABLE 7.  DATA FROM BAYOU  CHICO  BOTTLE  TEST,  ACTIVE WATER WITH SJP-4





 Hydrocarbon            Day 0         Day 1         Day  2         Day 4C       Day 8         Day  *



 Benzene                 9.6 (+_ .2)



 Cyclohexane            14.4 (+_ .1)



 2,3-Dimethylpentane    92.7 (_+ .2)



 3-Methylhexane         56.6 (+_ .2)



 Heptane               158.0 (+7.8)     -



 Methyl cyclohexane      81.0 (+_ .6)



 2,5-Dimethylhexane     19.8 (+6.3)     -



 2,4-Dimethylhexane     22.6 (+_ .5)     -



 Methylbenzene          69.5 (+1.5)     -



 2-Methyl heptane        69.0 (+13.1)    -



 3-Methyl heptane        61.5 (_+5.8)     -



 Octane                  49.2 (+_ .8)



 Ethylcyclohexane       65.0 (+_ .7)   1.0&           -



 Ethyl benzene            26.1 (+_!)-



 m-Xylene                54.7 (+1.9)   1.3 (+_ .3)



£-Xylene                34.5 (+_  1)    1.1 (+_  0)    -



_o-Xylene                54.0 (+1.1)    1.7 (± .2)                 -             -            4.Qb

-------
-p.
ro
         TABLE  7.   DATA  FROM  BAYOU  CHICO  BOTTLE  TEST,  ACTIVE  WATER  WITH SJP-4  (CONCLUDED)


Hydrocarbon            Day  0          Day  1         Day2         Day  4C        Day 8        Day 13

Nonane                 81.6 (±1.6)     8.6 (±2.4)    1.0 ( + .7)     -

Isopropyl benzene         2.5 (±  0)

1,3,5-Trimethylbenzene 53.0 (± .9)    12.1 (±1.9)    2.7 (± .3)     -

1,2,4-Trimethylbenzene   3.0 (+_ .9)     1.2 (±2.5)    3.8 (± .5)     -

Decane                 57.7 (+1.9)    48.3 (±5.8)   17.9 (± .1)    2.8

1,2,3-Trimethylbenzene 10.5 (± .2)     4.0 (± .7)    1.2 (± .1)     -

Indan                  18.3 (± .3)     8.1 (+_ .9)    2.6 (±  0)

Undecane               47.3 (±2.7)    13.4 (±5.6)   60.7 (±6.5)  135.8          4.3 (±4.9)

Naphthalene              9.9 (± .4)     5.4 (± .6)   12.6 (+ .9)    8.8          1.9 (+1.3)

Dodecane               51.2 (±2.9)     2.5 (±3.2)   94.3 (±10.2)   78.2        26.1 (±9.3)    0.5 (+_ .4)

Tridecane              45.0 (±2.7)     2.5 (±  2)   88.5 (± 12)   87.3         50.0 (±  5)    8.1 (±2.5)

Tetradecane            35.0 (±2.1)     4.8 (±1.1)   52.3 (±1.1)   55.6         42.2 (±2.5)   23.7 (±3.7)

Pentadecane            17.3 (± .7)     1.8 (± .7)   25.4 (±2.2)   38.2         21.2 (±1.1)   21.2 (±2.3)

Hexadecane	-	^	-	-	i	-

Concentrations  (mg/£)a of selected  hydrocarbons  in active water bottles from quiescent bottle test,
using water samples from  Bayou  Chico  and  shale-derived JP-4S

aAverage of replicate samples.
bBad replicate; n=l
cDay 4.  No duplicate sample.
Parentheses indicate one  standard deviation  from the mean.
Dashes (-)  indicate not  detectabel  (<0.2  mg/£).

-------
                TABLE  8.   DATA FROM BAYOU CHICO  BOTTLE TEST, STERILE SEDIMENT  WITH SJP-4

Hydrocarbon             Day 0         Day 1         Day 2        Day 4        Day 8        Day 13
Benzene                  4.3 (_+ .6)     -
Cyclohexane             11.5 (+_ .2)
2,3-Dimethylpentane     11.3 (+1.1)    2.6  (+_ .2)    3.7 (+ .1)     -          10.2b
3-Methylhexane          30.7 (+2.3)    1.7  (+_ .9)    2.3 ( + .1)     -            5.9b
Heptane                   -           11.2  (+4.4)   13.8 (+_1.2)    7.1 (+;  .7)  63.4 (^8.5)
Methylcyclohexane      36.1 (+2.4)    2.5  (+_ .2)    3.0 (+_ .7)    1.5 (+_  .4)
2,5-Dlmethylhexane      9.7 (+_ .7)
2,4-Dimethylhexane     15.2 (+1.3)     -            1.4 (+_  1)     -
Methylbenzene          26.4 (+2.6)    1.3  (+1.6)     -
2-Methyl heptane        14.8 (+1.1)    2.5  (+_ 0)    3.7 (+_ .1)    2.2 (+_  .6)    1.1  (+_ .1)
3-Methylheptane        40.3 (+_2.7)    2.4  (+ .1)    3.5 (+_ .1)    2.0 (+  .6)    1.3  (+ .5)
1,1-Dimethylcyclohexane 0.8 (+_ .1)    0.2b          -
Octane                 23.5 (+1.7)    2.0  (+_ .1)    3.0 (+_  0)    1.8 (+_  .5)    0.9  (+_ .1)
Ethyl cyclohexane       27.4 (+_1.8)    2.9  (^ .1)    4.7 (_+ .4)    2.3 (+_  .6)    1.3  (+_ .5)
Ethylbenzene           12.7 (+1.7)    1.0  (+_ .9)    1.0 (+_ .2)     -
jn-Xylene                29.6 (+2.7)    2.8  (+_ .9)    1.8 (± .5)     -
£-Xylene                13.6 (+2.1)    1.8  (+_ .8)    1.2 (+_ .8)     -
2-Xylene                23.7 (+1.9)    2.2  (+_ .7)    1.2 (+ .3)

-------
          TABLE  8.   DATA FROM BAYOU CHICO BOTTLE TEST, STERILE  SEDIMENT  WITH  SJP-4  (CONCLUDED)


Hydrocarbon             Day 0         Day 1        Day 2        Day  4         Day  8         Day 13

Nonane                  34.4 (^2.5)   16.2 (+_ .3)   6.7  (+_  .4)    3.9 (^1.6)    1.8 (+_ .7)

Isopropylbenzene         0.6 (+_ .2)

1,3,5-Trimethylbenzene 20.5 (+1.4)   10.0 (^ .2)   4.5  (+_  .7)     -

1,2,4-Trimethylbenzene 24.9 (+_1.4)    7.3 (+1.8)   5.7  (+1.7)

Decane                  49.7 (+4.7)   54.2 (+4.4)  16.3  (+_  4)    6.7 (+_1.6)    3.3 (+_ .5)    1.0  (+_ .5)

1,2,3-Trimethylbenzene  6.0 (+_ .6)    3.1 (+_ .7)   1.4  (+_  .7)     -

Indan                    7.0 (_+ .7)    6.5 (+_  1)   1.9  (+_  .8)     -

Undecane                61.4 (+4.4)   15.3 (+11.3)  50.1  (+8.7)  51.3 (+13)    4.6 (+_ .8)    1.8  (+ .7)

Naphthalene              8.4 (+_ .5)    6.5 (+JL.9)  12.3  (+_3.4)    5.7 (+_  .8)    0.5 (+_  0)

Dodecane                68.3 (+_  4)c  18.5 (+17.3)  78.1  (+_42.8) 53.9 (+7.1)   10.3 (+_ .2)    2.6  (+_  1)

Trldecane               61.8 (+_7.9)^  17.7 (+_ 18)  78.8  (+_45.5) 78.3 (+_7.9)   23.5 (+_ .1)    4.1  (+_ .8)

Tetradecane             47.1 (+2.1)c  13.7 (+11.8)  47.9  (+24.7) 46.9 (+   5)   36.3 (+1.3)    8.9  (+6.3)

Pentadecane             21.6 (+1.4)c  24.1 (+5.5)  21.8  (+11.3) 25.1 (+_1.7)   20.0 (+_  1)    9.3  (+3.9)

Hexadecane	-	-	-	-	-	-	

Concentrations  (mg/£)a of selected hydrocarbons in sterile sediment bottles  from quiescent bottle
test, using sediment  samples from Bayou Chico and shale-derived  JP-4.

aAverage of replicate  samples.
bBad replicate; n=l
cNo duplicate water samples.
Parentheses indicate  one  standard deviation from the mean.
Dashes (-) indicate not detectable (<0.2 mg/£).

-------
TABLE 9.  DATA FROM BAYOU CHICO BOTTLE TEST,  ACTIVE SEDIMENT WITH SJP-4
Hydrocarbon Day 0
Benzene
Cyclohexane
2,3-Dlmethyl pentane
3-Methyl hexane
Heptane 21
Methyl cyclohexane
2,5-Dimethyl hexane
2,4-Dimethyl hexane
Methyl benzene
2-Methyl heptane
3-Methyl heptane
1,1 -Dimethyl cyclohexane
Octane
Ethyl cyclohexane
Ethyl benzene
m-Xyl ene
£-Xylene
o-Xylene


1
2
1
3
0
1
3
2
5

3
4
1
6
1
4
-
-
.5
.0
.3
.5
.8
.1
.1
.6
.5
-
.6
.4
.3
.4
.1
.1


(±-
(± •
(+8.
(± •
(± •
(± •
(± •
(± -
(± •

(± -
(± -
(± •
(± •
(± •
(± -
Day 1 Day 2 Day 4 Day 8 Day 13
_
_
1) -
1) - 1.2 (+ 0) - 1.5 (+ .2)
1) - - 20.3 (+4.1)
2) - 1.4 (+_ 0) 1.7 (+_ .6) 1.4 (+_ .2)
1) -
1) -
2) -
1) - 1.7 (+_ .1) 2.1 (+_ .6) 2.5 (+ .7)
5) - 1.5 (+_ .1) 2.1 (+_ .7) 2.6 (+_ .7}
- - - - -
3) - 1.3 (+_ .1) 1.8 (_+ .5) 1.9 (+; .5)
5) 1.3 (+_ .3) 1.7 (+_ .2) 2.4 (+_ .6) 2.1 (+_ .6)
1) -
8) -
1) 0.8 (_+.!)-
4) 2.2 (+_ .2)

-------
          TABLE 9.   DATA FROM BAYOU CHICO BOTTLE  TEST,  ACTIVE  SEDIMENT WITH SJP-4 (CONCLUDED)


Hydrocarbon             Day 0         Day 1         Day  2         Day 4        Day 8        Day 13

Nonane                   8.3 (+_  1)    7.8  (+_  .5)    2.6 (+; .8)    3.0 (+; .6)    1.1 (+_  1)

Isopropylbenzene         -             _____

1,3,5-Trimethylbenzene  7.5 (+_!.!)   10.0  (_+  .1)    3.1 (+_ .2)    1.2 (_+ .3)

1,2,4-Trimethylbenzene  9.7 (+_  1)   25.0  (+_  .3)    4.4 (+_ .3)    1.1 (+_ .3)

Decane                  25.3 (+2.9)   92.0  (+_  .1)   13.9 (+_ .7)    6.0 (+ .9)    4.3 (j-  2)   0.8 (+ .2)

1,2,3-Trimethylbenzene  2.8 (+_ .4)    4.1  (+_.!)-

Indan                    3.5 (_+ .5)    6.8  (+_  .1)    1.7 (+_ .3)     -

Undecane                48.2 (+1.3)   76.6  (+1.3)   43.7 (+2.3)   25.9 (+9.1)    6.6 (+2.6)   1.2 (+_ .3)

Naphthalene              7.4 (+_ .3)   15.1  (+_  .9)    8.5 (+_ .6)    7.2 (+_2.5)    0.8 (+_ .3)

Dodecane                62.0 (+1.6)  107.0  (+6.5)   70.7 (+_3.6)   67.6 (^ 15)   13.4 (+_  5)   2.0 (+_ .9)

Tridecane               55.1 (+_  0)   91.0  (jf3.3)   75.5 (+4.6)   84.9 (+_10.2)  37.4 (+6.4)   3.8 (j+1.6)

Tetradecane             42.8 (+_ .5)   62.9  (+2.9)   43.4 (+2.1)   55.2 (+_3.6)   42.6 (+_  2)   9.3 (+_ 10)

Pentadecane             18.6 (_+ .3)   26.2  (+  0)   19.0 (_+ .2)   30.1 (^1.6)   23.5 (+_ .4)   8.1 (+_6.7)

Hexadecane	-	-	-	-	-	-	

Concentrations  (mg/£)a of selected hydrocarbons  in  active sediment bottles from quiescent bottle test,
using sediment  samples from Bayou Chico and shale-derived JP-4.

aAverage of  replicate  samples.
^Bad replicate;  n=l
Parentheses  indicate one  standard deviation from the mean.
Dashes (-) indicate not detectable (<0.2 mg/£) .

-------
                TABLE  10.   DATA  FROM  BAYOU CHICO BOTTLE TEST, ACTIVE WATER WITH PJP-4
Hydrocarbon



Benzene



Cyclohexane



2,3-Dimethylpentane



3-Methylhexane



Heptane



Methylcyclohexane



2,5-Dimethylhexane



2,4-Dimethylhexane



Methyl benzene



2-Methylheptane



3-Methylheptane
  Day Oc



  20.9 (+4.3)




  89.9 (+14.4)



  32.9 (+6.2)




  88.0 (+14.3)



2751.3 (+310.1)



  91.7 (+16.5)



  19.8 (+4.1)



  46.3 (+9.8)



  47.5 (+13.3)



 131.2 (+_25.3)



 160.3 (+32.4)
Day 1
Day 2
Day 4
Day 8
Day 13
 1,1-Dimethylcyclohexane 6.3  (+1.5)
Octane



Ethylcyclohexane



Ethyl benzene



jn-Xylene



_p_-Xylene



_o-Xyl ene
 216.4 (+41.1)



  56.8 (+13.2)



  28.5 (+8.9)



  54.4 (+17.7)



  36.2 (+10.5)



  35.3 (+11.3)

-------
                         TABLE  10.   DATA  FROM  BAYOU  CHICO  BOTTLE TEST,  ACTIVE WATER WITH PJP-4 (CONCLUDED)


               Hydrocarbon            Day Oc         Day 1         Day 2         Day 4        Day 8        Day 13

               Nonane                 132.4  (+34.3)   11.1 (+1.7)    1.4&

               Isopropylbenzene        4.0  (+_1.4)      -

               1,3,5-Trimethylbenzene 39.3  (+12.1)    9.1 (+1.1)    1.7 (+_ .8)     -

               1,2,4-Trimethylbenzene 52.2  (+17.3)   15.3 (+JL.2)    3.3 (+JL.5)

               Decane                 128.7  (+41.6)   50.7 (+4.8)   19.7 (+4.6)

               1,2,3-Trimethylbenzene 23.1  (+8.2)     3.4 (+_ .7)    2.3 (+_ .5)     -

               Indan                   8.4  (+3.3)     3.4 (+_ .2)    1.1 (+_ .3)     -

^              Undecane               153.2  (+_50.5)   99.2 (+_7.3)   68.9 (+.2.3)   51.2 (+2.4)    1.2 (+_ .6)
oo
               Naphthalene            32.1  (+9.4)    11.6 (+1.5)   21.5 (+2.3)    7.4 (+_ .2)    1.1 (+_ .5)

               Dodecane               150.9  (+54.5)    5.4 (+_  6)   96.0 (+_ .5)   55.5 (+1.6)   18.0 (+_5.5)

               Tridecane              133.4  (+48.3)   46.1 (+_2.9)   84.2 (+1.8)   77.7 (+_3.3)   37.7 (+7.2)    3.3 (+_  4)

               Tetradecane           100.5  (+34.6)   53.2 (+_2.5)   50.9 (+_ .8)   50.7 (+_  1)   35.3 (+.5.2)   13.5 (+_8.3)

               Pentadecane            36.2  (+11.3)   16.9 (+_ .2)   17.9 (+_ .1)   25.6 (+ .2)   14.3 (+1.6)   11.9 (+3.2)

               Hexadecane	2	I	     "	-	I	~	

               Concentrations (mg/£)a of  selected  hydrocarbons  in active water bottles from quiescent bottle test,
               using water samples from Bayou  Chico  and petroleum-derived JP-4.

               aAverage of replicate samples.
               bBad replicate; n=l
               cAverages recalculated from  repeated  test data;  standard deviations calculated  from
                repeated test data.
               Parentheses indicate one standard deviation from the mean.
               Dashes (-)  indicate not detected (<0.2 mg/S.) .

-------
                TABLE  11.   DATA  FROM  BAYOU CHICO BOTTLE TEST, STERILE WATER WITH  PJP-4
Hydrocarbon
Benzene
Cyclohexane
Day 0 Day 1 Day 2 Day 4 .PJLLJL
23.7 (+3.2) -
52.9 (+11.7) -
Day 13
-
2,3-Dimethylpentane   102.2  (+3.9)



3-Methylhexane          79.0  (+11.5)



Heptane               722.7  (+_332.2)



Methyl cyclohexane     102.9  (+12.2)



2,5-Dimethylhexane      22.7^



2,4-Dimethylhexane      33.6  (+6.4)



Methylbenzene           67.2  (+7.3)



2-Methylheptane       137.9  (+17.4)



3-Methyl heptane       153.8  (+21.6)



1,1-Dimethyl cyclohexane 0.3  (+_ .9)



Octane                253.4  (+_27.4)



Ethyl cyclohexane        70.4  (+_7.8)



Ethylbenzene            31.2  (+_4.7)



m-Xylene                60.0  (+_  9)



£-Xylene                42.7  (+_5.5)



o-Xylene                44.7  (+_5.9)     1.0 (+_ .1)

-------
                         TABLE  11.   DATA  FROM  BAYOU CHICO BOTTLE TEST,  STERILE WATER WITH PJP-4 (CONCLUDED)


               Hydrocarbon             Day 0          Day 1        Day 2         Day 4        Day 8        Day 13

               Nonane                  27.6 (+18.4)   10.7 (+1.9)    1.6 (j+1.1)

               Isopropylbenzene         7.3 (+_  .7)      -

               1,3,5-Trimethylbenzene  55.5 (+5.8)     8.6 (+_  1)    2.5 (±1.7)

               1,2,4-Trimethylbenzene  84.2b          14.8 (+1.4)    3.0 (+2.7)

               Decane                153.2 (+20.1)   49.7 (+4.9)   18.4(^11.5)    -

               1,2,3-Trimethylbenzene   4.1 (+.3.9)    5.9b         2.1 (+_ 1.3)

               Indan                   13.4&          3.6  (+_.2)    1.5 (+_!.!)

               Undecane                73.8 (+22.5)  113.2 (+6.8)   72.0(^18.9)  155.2 (+20.6)
o
               Naphthalene              7.1 (^3.1)     4.5 (+1.7)   21.7(+_ 3.9)    9.7 (+• .2)

               Dodecane                11.0 (+20.6)    3.9 (+.5.6)  102.7(+16.1)   61.7 (+1.2)    3.9 (^3.5)   0.5 (+_ .4)

               Trldecane                2.8 (+15.1)  108.3 (+_2.4)   95.3 (+.2.8)   77.0 (+_3.6)   21.5 (^9.6)   9.5 (+_2.1)

               Tetradecane             76.4 (+_11.7)   57.4 (+_1.4)   57.0 (+ .9)   50.8 (+28.8)  29.9 (+6.5)  15.9 (+_3.2)

               Pentadecane              1.2 (+4.7)    18.8 (+_ .4)   19.4 (+_ .6)   34.7 (+22.9)  14.4 (+_2.4)  14.3 (^1.5)

               Hexadecane	-	-	-	-	-	-	

               Concentrations (mg/Ji)a  of  selected  hydrocarbons  in sterile water bottles from quiescent bottle test,
               using water samples from Bayou  Chico and petroleum-derived JP-4.

               aAverage of replicate samples.
               ^Bad replicate; n=l.
               Parenthesis indicate one standard deviation from the mean.
               Dashes (-)  indicate not detectable  (<0.2 mgA) .

-------
              TABLE 12.  DATA FROM BAYOU  CHICO  BOTTLE  TEST,  STERILE SEDIMENT WITH PJP-4
Hydrocarbon
Benzene
Cyclohexane
2,3-Dimethyl pentane
3-Methylhexane
Heptane
Methyl cycl ohexane
2,5-Dimethyl hexane
2,4-Dimethyl hexane
Methyl benzene
2-Methyl heptane
3-Methyl heptane
Day 0
9.9 (± ,1}
31.0(±12.3)
21.7 (+11)
30.7 (±2.8)
_c
34.0(^15.7)
10.2 (± 1)
20.7 (+2.2)
24.2 (±2.1)
64.2 (±7.6)
78.5 (4-9.5)
Day 1
-
-
-
-
161.2(±57.7)
1.1 (± .2)
-
-
1.1 (± .1)
2.1 (±1.3)
2.8 (+1.7)
Day 2
-
-
-
2.7 (+2.5)
40.7(4-25.1)
4.1 (+,3.2)
-
-
-
7.1 (+4.7)
5.2 (±5.5)
Day 4
-
-
-
1.6 ( + .8)
24.8(±10.4)
2.1 (±1.1)
-
-
-
4.2 (±1.9)
5.1 (±2.2)
Day 8 Day 13
-
-
-
-
12.38(±13.3) 25.3 (±4.1)
1.6 (± .8)
-
-
-
3.9 (±1.9) 1.8 (± .5)
6.1 (±2.3) 2.8 (± .7)
1,1-Dimethyl cycl ohexane 2.6 (+ .4) -
Octane
Ethyl cycl ohexane
112.1(^13.7)
28.8 (+3.6)
4.9 (±2.9)
1.1 (± .5)
15.3 (±9.6)
4.4 (±2.6)
8.9 ( + 3)
2.3 (± .9)
8.3 (±3.3) 3.7 (± .8)
1.9 (± .8) 0.6 (± 0)
Ethylbenzene            14.1  (±1.5)     0.9 (+_ .2)



m-Xylene                26.1  (±6.8)     1.8 (±1.1)    3.1  (±1.7)    1.1 (± .2)



_p_-Xylene                20.6  (±1.8)     1.0 (± .3)



o-Xylene                19.1  (±1.6)     0.9 (± .3)

-------
        TABLE 12.  DATA FROM BAYOU CHICO BOTTLE TEST,  STERILE  SEDIMENT WITH PJP-4 (CONCLUDED).
Hydrocarbon
Nonane
Isopropyl benzene
1 ,3,5-Trimethylbenzene
1 ,2,4-Trimethyl benzene
Decane
1,2,3-Trimethyl benzene
Indan
Undecane
Naphthalene
Dodecane
Tridecane
Tetradecane
Pentadecane
Hexadecane
Concentrations (mgA)a
quiescent bottle test,
Day 0
68.2
2.1
20.5
28.7
63.9
13.4
4.2
72.6
16.4
70.0
56.8
42.0
15.2
_
(+8.6)
(± .1)
(±2.6)
(±2.9)
(±8.5)
(+1.4)
(± .5)
(±9.5)
(± .9)
(±8.8)
(±+.5)
(±3.8)
(±1.7)

Day 1
6.0 (±2.2)
-
3.3 (+_ 1)
5.3 (±3.4)
20.6(±10.7)
3.7 (+_ 1)
0.9 (± .2)
45.2(±12.7)
11.1 (±3.9)
51.7 (± 15)
45.5 (± 12)
34.2 (±8.1)
11.8 (±2.9)
-
of selected hydrocarbons in
using sediment samples from
Day 2
11.8
-
4.0
6.6
18.8
3.4
0.8
57.4
19.8
85.1
78.2
48.6
16.8
-
(±6.6)

(±1.9)
(± 3)
(±5.8)
(±1.1)
(± .1)
(±7.2)
(±1.8)
(±6.7)
(±5)
(±2.4)
(±1.2)

Day
6.3
-
1.8
1.0
6.2
-
-
41.8
6.8
45.7
58.5
36.3
16.0
-
sterile sediment
Bayou Chico
and
4_
(±1.7)

(± -5)
(± -3)
(±1.1)


(±9.1)
(± 2)
(±8.6)
(±3)
(± .7)
(± .8)

bottles
Day £
5.4
-
-
-
4.9
-
-
6.0
0.7
8.5
18.9
27.4
12.3
-
from
!
(±2



(±1


(±
(±
(±1
(±9
(±5
(±2


petrol eum-deri ved
Day 1
.2) 2.4
-
-
-
.4) 2.3
-
-
3) 3.2
.2)
.5) 3.6
.8) 3.5
.5) 7.5
.4) 6.1
_
JP-4.
3
(+ .5)



(± .5)


(± -5)

(± -7)
(± -4)
(±6.5)
(± 4)


aAverage of replicate samples.
bBad replicate; n=l.
clnterferences prevent accurate integration.
Parentheses indicate  one standard deviation from the  mean.
Dashes (-)  indicate not detectable (<0.2 mgA) .

-------
               TABLE  13.   DATA  FROM BAYOU CHICO BOTTLE TEST, ACTIVE SEDIMENT  WITH  PJP-4




Hydrocarbon            Day 0          Day 1        Day 2        Day 4        Day 8         Day 13



Benzene                   -             -


Cyclohexane              3.3 (± .8)



2,3-Dlmethylpentane      1.1 (± .3)      -            -           2.2 (± .4)


3-Methylhexane           4.1 (+1.8)     1.2 (±1.2)   1.5 (± .2)   1.7 (± .3)    2.9 (+1.5)



Heptane                336.3(±50.1)    16.7(^29.6)  18.7 (±4.5)  11.9 (± .2)  117.6(^66.1)   23.6 (  ± 5)



Methyl cyclohexane        5.7 (± .7)     3.4 (±1.4)   2.2 (+_ .9)   2.0 (± .4)    2.4 (+1.3)



2,5-Dlmethylhexane       1.1 (± .2)


2,4-Dimethylhexane       2.1 (+  .3)      -
                              —

Methyl benzene            3.6 (± .3)


2-Methyl heptane          9.3 (±1.2)     3.5 (+1.4)   3.8 (+1.3)   3.6 (+  .5)    5.7 (±3.2)    1.5 (± .2)


3-Methyl heptane         12.0 (+1.1)     4.4 (^2.1)   3.1 (+_!.!)   4.6 (+_ .4)    7.7 (±4.3)    1.8 (+ .2)



1,1-Dimethylcyclohexane   -             -


Octane                  18.2 (+_ .9)     8.3 (±3.4)   8.4 (+_  2)   8.3 (+  .2)  11.3 (+5.7)    2.7 (± .3)



Ethyl cyclohexane         4.9 (± .1)     5.5 (+_ .7)   2.3 (+_ .8)   2.2 (+_ .1)    2.6 (+1.5)



Ethylbenzene            2.2 (± .1)     3.6 (+_ .3)


m-Xylene                 -            1.3 (+_ .4)   1.0 (±1.5)   1.3 (± 0)     -


£-Xylene                8.5 (±1.3)     1.5 (± .3)    -            -            0.9 (± .5)


o-Xylene                3.7 (+ .7)     1.7 (+ .2)

-------
                       TABLE  13.   DATA  FROM  BAYOU  CHICO BOTTLE TEST, ACTIVE SEDIMENT WITH PJP-4 (CONCLUDED).
on
-Pi
Hydrocarbon
Nonane
Isopropylbenzene
1,3,5-Trimethyl benzene
1, 2, 4-Tri methyl benzene
Decane
1, 2, 3-Tri methyl benzene
Indan
Undecane
Naphthalene
Dodecane
Tridecane
Tetradecane
Pentadecane
Hexadecane
Day Q
14.6 (4-
0.5 ( +
7.1 (+_
11.8 (±
29.4 (±
7.1 ( +
1.7 (±
54.8 (±3
14.0 (±
60.4 (±1
51.9 (±1
38.3 (±1
13.1 (±
-

.2)
.1)
0)
.5)
.8)
0)
.1)
.7)
.3)
.6)
.6)
.3)
.7)

Day 1
17.0 (±
-
9.6 (±
26.0 (±
116.1 (±
8.7 (±
2.9 (±
87.0 (±
25.9 (±
101.0 (±
86.3 (±2
54.5 (±
17.0 (±
-

1)

.1)
0)
0)
.1)
-1)
.1)
•2)
.2)
.9)
.5)
.2)

Day 2
5.9
-
2.2
3.2
11.8
2.0
-
42.1
14.3
67.5
64.7
40.7
13.4
-

(±1.3)

(± -3)
(± -4)
(± -3)
(± .1)

(±1.7)
(±1.1)
(±4.1)
(±6.9)
(±2.7)
(±1.2)

Day
5.9
-
1.3
1.0
5.5
-
-
14.5
6.7
48.0
63.6
44.3
20.2
-
£
(± .2)

(± 0)
(± -2)
(± .2)


(±1.1)
(± -8)
(±3.4)
(+3.9)
(± 2)
(+1.1)

Day {
6.4
-
1.1
-
5.4
-
-
6.6
0.8
7.3
15.4
25.5
12.2
-
I
(+3.1)

(± -6)

(+2.6)


(±3.2)
(± -4)
(+2.9)
(± 4)
(± .6)
(± -7)

Day 13
1.6 ( 0)
-
-
-
1.4 ( .1)
-
-
2.1 ( .5)
-
2.5 ( .4)
2.9 ( 1.1)
7.2 ( 8.2)
5.3 ( 4.6)
-
              Concentrations (mg/£)a of  selected hydrocarbons in active sediment bottles from quiescent bottle test,
              using sediment samples from Bayou Chico and petroleum-derived JP-4.
              aAverage of replicate samples.
              bBad  replicate; n=l
              Parentheses indicate one standard deviation from the mean.
              Dashes  (-) indicate not detectable  (<0.2 mgA).

-------
                           TABLE 14.   COMPARISON OF DEGRADATION RATES IN THE BAYOU CHICO TEST
Hydrocarbon
Methyl cycl ohexane
Ethyl cyclohexane
Ethyl cycl ohexane
p-Xylene
en
en
Hydrocarbon
Decane
Ethyl cycl ohexane
Ethyl cycl ohexane
Dodecane
Source
Shale
Shale
Petroleum
Shale
Sample
Steril e
Sterile
Active
Steril e
Sample
Type
Sediment
Sediment
Sediment
Sediment
Type
water
sediment
sediment
water
Sterile
Confidence
Ratefh'1) Limits
-.0118 +.0065 to -.0300
-.0048 +.0006 to -.0101
-.0032 +.0004 to -.0067
-.0035 +.0177 to -.0246
Shale-derived
Confidence
Rate(h-1) Limits
-.018 +.004 to -.040
-.005 +.001 to -.010
-.0003 +.0030 to -.0035
-.0056 +.0014 to -.0096

Rateslh'1)
-.0008 +.
-.0003 +.
-.0015 +.
-.0008 +.
Petrol
Rates(h-1)
-.019 +.
-.003 +.
-.0015 +.
-.0047 +.
Active
Confidence
Limits
0275 to -.0290
003 to -.0035
001 to -.0039
0275 to -.029
eum derived
Confidence
Limits
004 to -.034
0004 to -.0067
001 to -.0039
0006 to -.0099
Significant
Difference
None
None
None
None
Significant
Difference
None
None
None
None
Comparison of rates of disappearance of selected hydrocarbons  in  shale-derived  and  petroleum-derived  jet  fuels  from
quiescent bottle tests containing water and sediment from Bayou  Chico  relative  to  sterile  and  active  systems  (top)  and
fuel types (bottom).

-------
than higher boiling ones.  No significant difference in  disappearance rates



was noticed between SJP-4 and PJP-4 (Table 23).



        Subsequent tests with radiolabeled substrates indicated that mineral-



ization of hydrocarbons to C02 was occurring (Figure 17).



D.  TOXICITY TESTING



    The results of our toxicity testing are presented in  Figure 18.   The test



results clearly indicate a toxic effect as a result  of exposure to SJP-4.



Toluene was mineralized by the substrate, but the  addition  of SJP-4  to the



environmental  sample resulted in almost no C02 production  indicating a



toxic effect.



E.  DISSOLVED ORGANIC CARBON



    Results from quiescent bottle tests in which  SJP-4 and  PJP-4 were in-



cubated with water samples from several locations  showed  unexplained vari-



ability in hydrocarbon evaporation rates.  We hypothesized  that variations



in DOC from one sample to another may be responsible for  the  variations  in



the evaporation rates observed in our experiments  because  hydrocarbons evap-



orated less rapidly when dissolved in water than  when incorporated into  a



surface slick.



    Hydrocarbon solubility increased with the addition of DOC as evidenced



by decreasing evaporation rates (greater persistence in  sterile systems)



with increasing DOC concentrations (Figure 19).   The increase in solubility



of alkanes was approximately proportional to DOC  concentrations at both



24 and 48 hours.  The solubilities of aromatic compounds  were similarly



affected (Figure 20).



F.  Jet Fuel  Evaporation Rate



    Ninety percent of the SJP-4 evaporated within 6  days  (Figure 21).  This



represents an  idealized situation since, in the field, wind currents will





                                    56

-------
              TABLE  15.   DATA  FROM  ESCAMBIA RIVER BOTTLE TEST, STERILE WATER WITH  SJP-4
Hydrocarbon
Benzene
Cyclohexane
2,3-Dlmethyl pentane
3-Methylhexane
Day 0 Day 1 Day 2 Day 4 Day 8
4.2 (+2.4) -
15.5 (+0.4) -
75.4 (+0.3) -
33.5(+13.2) - 11.3 (+9.6)
Day 12
-
-
-
-
Heptane               487.3(+82.0)   324.5(+_19.2)  181.2(+_68.9) 167.1(^11.5)  57.5(^12.7)



Methylcyclohexane       50.5  (+1.9)



2,5-Dimethylhexane      17.4  (+_0.0)      -



2,4-Dimethylhexane      36.0  (+0.4)      -



Methylbenzene           16.4  (+0.2)      -



2-Methylheptane         50.5  (+1.4)      -



3-Methylheptane         34.7(^15.6)      -



1,1-Dimethylcyclohexane 1.3  (+0.0)



Octane                  50.4(+_24.6)      -



Ethylcyclohexane        38.3  (+1.4)      -



Ethylbenzene           10.5  (+_2.6)      -



ni-Xylene                28.6  (+1.6)



£-Xylene                18.3  (+_0.2)     0.3b          -



o-Xylene                22.8  (+7.4)      -           2.7 (+4.5)   3.7 (+0.1)   3.8  (+0)

-------
                       TABLE  15.   DATA  FROM  ESCAMBIA  RIVER  BOTTLE  TEST,  STERILE WATER WITH SJP-4 (CONCLUDED).
en
CO
Hydrocarbon
Nonane
Isopropylbenzene
Day (
42.7
1.1
)
(±2.5)
(±0.6)
Day 1 Day 2 Day 4
1.9 (±0.2)
Day 8 Day 12
-
               1,3,5-Trimethylbenzene  24.5  (±1.2)     2.3  (±1.6)

               1,2,4-Trimethylbenzene  27.5  (±1.9)     4.9  (±0.3)   0.6 (+_  0)

               Decane                  50.3(±10.8)    17.2  (±8.5)   5.9 (±1.0)   0.!

               1,2,3-Trimethylbenzene   6.5  (+0.4)     2.1  (+0.9)
Indan
Undecane
NapHthalene
Dodecane
Tridecane
Tetradecane
Pentadecane
Hexadecane
7.
69.
12.
76.
62.
49.
22.
-
6
6
7
0
6
6
it

(±0.3)
(±2.8)
(±2.9)
(±0.9)
(±2,6)
(±1.5)
>

2.7
56.0
9.2
75.1
71.6
59.3
26.3
-
(±0.1)
(±4.1)
(±0.7)
(±5.2)
(±9.7)
(±4.8)
(±2.6)

0.
45.
9 =
72.
78.
54.
46.
-
8 (+0.3)
2 (+8.2)
5 (±1.0)
8(±10.9)
0(±10.8)
8 (+8.5)
4 (+5.7)

-
16.5
4.1
46.4
57.7
49.1
20.2
-

(±4.5)
(±0.6)
(±2.9)
(±0.7)
(±3.4)
(±1.2)

.-
-
-
2.3 (+1
22.0 (+_9
42.4 (+1
21.5 (+2
-
-
-
-
.8)
.8)
.9)
.5)
-
              Concentrations  (mgA)a of selected  hydrocarbons in sterile water bottles from quiescent bottle test,
              using water samples from Escambia River and share-derived JP-4.

              aAverage of replicate samples.
              ^Bad replicate; n=l
              Parentheses indicate one standard deviation from the mean.
              Dashes (-) indicate not detectable  (<0.2 mgA) .

-------
                              TABLE 16.  DATA FROM ESCAMBIA RIVER BOTTLE  TEST,  ACTIVE  WATER WITH SJP-4
01
Hydrocarbon



Benzene



Cyclohexane



2,3-Dimethylpentane



3-Methylhexane



Heptane



Methylcyclohexane



2,5-Dlmethylhexane



2,4-Dlmethylhexane



Methyl benzene



2-Methylheptane



3-Methy"! heptane
 Day 0



  5.7 (+0.2)



 14.4 (+0.4)




 72.8 (+0.3}



 40.6 (+0.7)




481.6 (+1.3)



 50.0 (±0.1)



 16.1 (+0.1)



 20.6 (+0.2)



 31.2 (+1.3)



 48.8 (+0.9)



 47.4 (+0.8)
               1,1-Dimethylcyclohexane 1.3  (+_  0)
               Octane



               Ethylcyclohexane



               Ethyl benzene



               m-Xylene



               _p_-Xylene



               o-Xylene
                        32.9  (+0.6)



                        38.4  (+1.5)



                        13.4  (+0.7)



                        28.7  (+1.8)



                        18.4  (+1.0)



                        28.1  (+1.8)
                                                    Day 1
Day 2
Day 4
Day 8
Day 12
                                                                                            14.6 (+ .2)

-------
                       TABLE  16.   DATA  FROM  ESCAMBIA  RIVER  BOTTLE  TEST, ACTIVE WATER WITH SJP-4 (CONCLUDED).
CT>
O
Hydrocarbon
Nonane
Isopropyl benzene
1, 3, 5 -Tri methyl benzene
1, 2, 4-Tri methyl benzene
Decane
1,2, 3-Trimethyl benzene
Indan
Undecane
Napthalene
Dodecane
Tridecane
Tetradecane
Pentadecane
Hexadecane
Day
46.
1.
25.
28.
63.
7.
8.
74.
11.
81.
70.
50.
23.
-
:_c
5
i
4
8
4
4
8
5
4
5
4(
7
4

)
(±2
(±0
(±1
(±2
(±4
(±0
(±0
(±5
(±1
(±6
±10
(±5
(±2

.5)
.6)
.7)
.1)
.4)
.6)
.7)
.9)
.0)
.8)
.2)
.0)
.3)

Day
1.
-
3.
3.
18.
1.
2.
47.
7.
62.
56.
46.
21.
-
4

0
8
5
*
1
!_
(±1.2)

(±1.9)
(±2.4)
(±8.6)
(±0 . 8)
(±1.2)
0(±10.6)
1
2
9
0
5

(±1.3)
(±8.0)
(±6.4)
(±4.0)
(±1.7)

Day 2
-
0.4
0.5
7.2
0.5
0.5
42.5
8.2
67.3
68.1
49.0
31.9
-

(±0.5)
(±0.7)
(±1.9)
(± 0)
(±0.3)
(±2.9)
(±0.1)
(±0.1)
(±5.6)
(±0.9)
(±0.8)

Day 4
-
-
-
0.5 (±
-
-
15.5 (±0.
4.2 (±0.
44.1 (±0.
50.5 (±1.
40.9 (±0.
Day 8 Day 12
-
-
-
0)
_
-
3)
1) 0.2 (± .4)
8) 7.4 (±6.3)
7) 33.6(±11.6)
3) 44.1 (± 6)
16.7 (±0.1) 21.5 (±1.9)
-
-
              Concentrations  (mg/£)a of selected  hydrocarbons in active water bottles from quiescent bottle test,
              using water samples from Escambia River and  shale-derived JP-4.

              aAverage of replicate samples.
              DBad replicate; n=l
              Parentheses indicate one standard deviation  from the mean.
              Dashes (-) indicate not detectable  (<0.2 mg/£).

-------
   TABLE 17.  DATA FROM ESCAMBIA  RIVER  BOTTLE TEST, STERILE WATER FROM SEDIMENT  SAMPLES  WITH SJP-4
Hydrocarbon
Benzene
Cyclohexane
2,3-Dimethylpentane
3-Methylhexane
Day 0 Day 1 Day 2 Day 4C Day 8
5.1 (+0.2) -
12.3 (+0.5) -
64.7 (+_2.6) -
36.3 (+1.4) 24.8 (+1.8) 28.7 (+1.5)
Day 12
-
-
-
-
Heptane               472.6(^15.9)   286.7(+29.2)  204.1(^78.5)  189.9         67.0(^16.7)



Methylcyclohexane      44.9  (+1.7)     0.4 (+0.1)     -



2,5-Dimethylhexane     14.3  (+0.6)      -



2,4-Dlmethylhexane     18.2  (+0.7)      -



Methylbenzene          28.7  (+1.0)      -



2-Methyl heptane        44.5  (+1.9)     4.1 (+0.2)    2.5 (+0.8)    2.2          0.7 (+_  1)



3-Methyl heptane        43.4  (+2.0)     3.7 (+0.1)    2.4 (+0.8)    2.0          0.8 (+1.1)



1,1-Dimethylcyclohexane  1.1  (+0.1)



Octane                 30.4(+_1.0)      2.6 (+0.2)    1.6 (+0.6)    1.5



Ethyl cyclohexane       35.3(+1.4)      3.3 (+0.1)    1.9 (+_0.7)    2.1          0.1 (+_  1)



Ethylbenzene           10.4(^3.0)      0.6 (+_0.1)     -



£-Xylene               27.2(+_1.0)      0.8 (+0.1)



2-Xylene               16.4  (+_0.6)     0.9 (+0.1)    0.8 (+0.1)    0.5



o-Xylene               26.1  (+0.6)     0.9 (+0.2)     -

-------
                  TABLE  17.   DATA  FROM  ESCAMBIA RIVER BOTTLE TEST, STERILE WATER FROM SEDIMENT SAMPLES WITH SJP-4
                             (CONCLUDED).
dh
Hydrocarbon
Nonane
Isopropyl benzene
1 , 3, 5 -Trl methyl benzene
1 , 2, 4-Tri methyl benzene
Decane
1,2, 3-Trimethyl benzene
Indan
Undecane
Naphthalene
Dodecane
Trldecane
Tetradecane
Pentadecane
Hexadecane
Day 0
42.7 (+1.4)
1.2 (+0.0)
23.0 (+0.6)
26.6 (+0.6)
56.2 (+0.1)
6.6 (+0.1)
7.6 (+0.1)
66.0 (+0.4)
9.2 (+0.6)
70.3 (+0.5)
61.5 (+1.6)
45.1 (+2.2)
21.0 (+1.3)
Concentrations (mg/£)a of selected
test, using sediment samples from
Day 1
6.2 (+0.9)
-
5.6 (±1.2)
6.9 (+2.1)
24.5 (+4.7)
1.9 (+0.5)
2.9 (+0.9)
50.3 (+8.1)
7.7 (+2.0)
67.7(+11.2)
63.7 (+.4.2)
48.6 (+4.3)
23.0 (+2.1)
hydrocarbons
Escambia River
Day 2
2.9 (+1.1)
-
1.7 (+.0.6)
1.6 (+0.6)
8.3 (+.2.4)
-
0.8 (+0.3)
28.8 (+7.9)
4.7 (+1.5)
42.7(+ll.l)
41.2 (+8.2)
30.2 (+7.4)
17.3 (+4.3)
Day 4C
2.9
-
-
0.6
4.1
-
-
15.5
3.8
42.7
61.5
49.7
22.4
in sterile sediment bottles
and shale-deri
ved JP-4.
Day 8 Day 12
1.1 (jf 1.5)
-
-
-
2.1 (±1.9)
-
-
3.1 (+2.6)
-
5.0 (+1.4)
18.7(^10.2)
34.5(+_12.6)
19.5(± 5.1)
from quiescent bottle
              aAverage of replicate samples.
              t>Bad replicate; n=l
              C0ay 4 - no duplicate sample.
              Parentheses indicate one standard deviation from the mean.
              Dashes (-) indicate not detectable (<0.2 mgA) .

-------
             TABLE  18.   DATA FROM ESCAMBIA RIVER BOTTLE TEST,  ACTIVE  SEDIMENT WITH SJP-4





Hydrocarbon             Day  0         Day 1        Day 2         Day  4         Day 8        Day 12



Benzene                  5.0 (+0.1)      -



Cyclohexane             11.7 (+0.2)



2,3-Dimethylpentane     59.5 (+0.2)      -



3-Methylhexane          33.8 (+1.0)      -           1.3 (+1.8)



Heptane                408.2(+_15.9)      -          14.1(+13.1)



Methylcyclohexane       42.1 (+1.7)



2,5-Dimethylhexane      13.3 (+0.3)      -



2,4-Dimethylhexane      17.3 (+0.9)      -



Methyl benzene           28.2 (+0.1)      -



2-Methyl heptane         39.9 (+3.9)      -           0.9 (+3.2)



3-Methyl heptane         41.7 (+2.2)     1.8 (+.1.4)   2.4 (+.6.4)



1,1-Dimethylcyclohexane 1.0 (+.0.1)



Octane                  28.9 (+2.2)      -           2.0(+_36.5)



Ethyl cyclohexane       34.1 (+2.4)     1.6 (+1.3)   1.6 (+.1.8)



Ethyl benzene           10.2 (+.2.0)      -



rri-Xylene               28.5 (+0.2)



£-Xylene               14.8 (+.2.2)      -



o-Xylene               24.3 (+.3.2)

-------
       TABLE  18.   DATA  FROM  ESCAMBIA RIVER BOTTLE TEST,  ACTIVE SEDIMENT WITH SJP-4 (CONCLUDED).


Hydrocarbon             Day 0         Day 1        Day 2         Day 4        Day 8        Day 12

Nonane                  41.7  (4-3.3)     3.3 (±1.6)    2.3 (±2.4)

Isopropylbenzene         1.1  (+0.2)      -

1,3,5-Trimethylbenzene  23.0  (±1.2)     3.8 (+0.6)    1.2 (±1.8)

1,2,4-Trimethylbenzene  27.3  (±1.3)     6.6 (+0.2)    1.4 (+2.2)

Decane                  57.1  (+4.1)    20.2 (±0.4)    4.8 (±  5)    2.3 (±2.4)    0.9 (± 2)

1,2,3-Trimethylbenzene   6.7  (+0.6)     1.5 (+0.1)

Indan                    7.8  (+0.6)     2.4 (±0.1)     -

Undecane                66.9  (+.6.7)    47.9 (+1.6)   16.1 (±9.4)    7.1 (+4.2)    1.5 (±1.1)

Naphthalene              8.8  (±2.0)     7.3 (±  0)    3.7 (±  1)    2.3 (± .3)    0.5 (+• .3)

Dodecane                75.6  (±7.8)    65.7 (+5.4)   31.9(+_10.4)   29.4 (+4.8)   11.0 (+4.2)

Tridecane               63.8  (±4.3)    66.8 (±6.0)   36.5 (±9.5)   48.7 (±5.9)   35.3 (±3.6)

Tetradecane             49.2  (±2.1)    52.5 (±3.7)   28.3 (±7.7)    40.1 (±1.9)  39.1 (± .7)

Pentadecane             21.9  (±1.0)    24.6 (±1.6)   12.4 (±4.2)    18.1 (±1.3)  19.5 (± .4)

Hexa-decane	-	-  	-	-	-	-	

Concentrations (mg/£)a  of selected  hydrocarbons  In active sediment bottles from quiescent bottle test,
using sediment samples  from  Escambia  River and shale-derived JP-4.

aAverage of replicate samples.
bBad replicate; n=l
Parentheses indicate one standard deviation from the mean.
Dashes (-) indicate not detectable  (<0.2 mg/£).

-------
                              TABLE  19.   DATA  FROM ESCAMBIA RIVER BOTTLE TEST, ACTIVE WATER WITH PJP-4
Ol
en
Hydrocarbon


Benzene


Cyclohexane


2,3-Dimethylpentane


3-Methylhexane


Heptane


Methylcyclohexane


2,5-Dlmethylhexane


2,4-Dlmethylhexane


Methyl benzene


2-Methylheptane


3-Methylheptane


1,1-Dimethylcyclohexane  4.3  (+0.2)


Octane                 170.0  (+4.0)


Ethylcyclohexane       36.9  (+8.1)
  Day 0


  13.6 (+0.8)


  52.9 (+5.3)


  76.5 (+2.2)


  56.4 (+2.8)


2110.8(+37.0)


  63.0 (+1.6)


  18.5 (+0.4)


  30.3 (+0.1)


  28.9 (+0.4)


  97.6 (+1.4)
               Ethyl benzene


               ni-Xylene


               jj-Xylene


               o-Xylene
  15.7 (+0.7)


  27.3 (+6.3)


  21.0 (+2.8)


  20.5 (+3.8)
                                                    Day 1
Day 2
Day 4
Day 8
Day 12
                                                                                           14.5  (+  .1)

-------
                       TABLE 19.  DATA FROM ESCAMBIA RIVER  BOTTLE  TEST,  ACTIVE  WATER  WITH  PJP-4  (CONCLUDED).
CTi
Hydrocarbon
Nonane
Isopropyl benzene
1 , 3,5-Trimethyl benzene
1,2, 4-Tri methyl benzene
Decane
1,2,3-Trimethyl benzene
Indan
Undecane
Naphthalene
Dodecane
Tridecane
Tetradecane
Pentadecane
Hexadecane
Concentrations (mg/£)a
Day
83.
2.
21.
28.
78.
16.
4.
84.
18.
73.
62.
48.
17.
_
of

8
7
4
3
8
3
6
9
3
3
5
1
8

0
(+19
(+0
(+6
(±7
(±5
(±2
(±1
(+6
(±o
(±5
(±1
b
b


-8)
.2)
.9)
.4)
.6)
-0)
-0)
• 1)
.2)
.6)
.6)



selected
Da
3

3
5
26
3
1
60
12
66
56
43
16

JLJ
.3
-
.4
.1
.6
.2
.3
.2
.3
.6
.8
.0
.0
-
L_
(+0.

(+0.
(+0.
(+1.
(+p.
(±
(+1.
(+0.
(+2.
(+0.
(+0.
(+0.


3)

3)
6)
3)
2)
0)
8)
2)
0)
9)
4)
2)

hydrocarbons
Day 2
-
-
-
-
4.3
0.2
-
40.0
9.7
59.6
60.1
44.5
23.0
-
in acti





(I1
(+0

(+5
(±1
(+6
(+4
(+3
(+2

ve
Day 4 Day 8 Day 12
_
_
_
_
.4) -
.3)
_
.8) 5.9 (+1.8)
.7) 3.1 (+0.3)
.7) 30.4 (+1.5) 0.5 (+_ .6)
.0) 40.5 (+0.7) 10.5 (+,2.4)
.2) 34.2 (+1.0) 27.7 (+1.4)
.1) 11.7 (+,0.6) 13.0 (+_ .1)
-
water bottles from quiescent bottle test.
               using  water  samples  from Escambia  River  and  petroleum-derived  JP-4.

               aAverage  of  replicate  samples.
               bBad  replicate;  n=l
               Parentheses  indicate one standard  deviation  from  the  mean.
               Dashes (-) indicate  not  detectable (<0.2 mg/£).

-------
              TABLE 20.  DATA FROM  ESCAMBIA  RIVER  BOTTLE TEST, STERILE WATER WITH PJP-4
Hydrocarbon
Benzene
Cyclohexane
2,3-Dimethylpentane
3-Methylhexane
Day 0 Day 1
14.3 (+2.6)
60.2 (+4.0)
85.0 (+_8.6)
61.2 (+5.9)
Day 2 Day 4 Day 8 Day 13
23.7 (+0.1)
Heptane             2,310.0(+292.3)  322.1(^26.1)  212.1 (+7.0)  142.6(+15.5)  50.9(+11.1)



Methylcyclohexane      65.2  (+9.2)



2,5-Dlmethylhexane     18.5  (+3.0)      -



2,4-Dimethylhexane     30.8  (+4.7)      -



Methyl benzene          27.7  (+6.3)      -



2-Methyl heptane        94.3(+_16.4)      -



3-Methylheptane        114.2(^21.6)      -             -           0.4^



1,1-Dimethylcyclohexane  4.0  (+0.8)      -



Octane                 160.8(+_31.7)      -             -           0.9 (+0.3)



Ethyl cyclohexane       38.8  (+_8.1)      -



Ethylbenzene           14.5  (+3.4)      -



m-Xylene               27.9  (+_6.9)      -



2-Xylene               20.5  (+_4.7)      -



o-Xylene               21.5  (+5.2)      -            4.1 (+_0.3)     -           4.0 (+•  .6)

-------
CTi
CO
         TABLE  20.   DATA  FROM ESCAMBIA RIVER BOTTLE TEST, STERILE WATER WITH PJP-4  (CONCLUDED).


Hydrocarbon            Day 0         Day 1        Day 2        Day 4        Day 8        Day  13

Nonane                 85.2(+19.1)     1.4 (+_ .4)     -           0.6 (j+0.2)

Isopropylbenzene         2.5 (+0.6)      -

1,3,5-Trimethylbenzene 22.9 (+5.8)     1.8 (+0.4)    0.2 (+0.3)

1,2,4-Trimethylbenzene 29.0 (+7.8)     3.1 (+0.8)    0.4 (+0.6)

Decane                 71.9(+17.4)    19.4 (+3.0)    6.2 (+4.6)    0.4b

1,2,3-Trimethylbenzene 12.9 (+_3.3)     2.3 (+0.4)    0.5 (+0.6)     -

Indan                    4.7 (+1.4)     0.9 (+0.1)    0.2 (+0.3)

Undecane               77.0(^17.2)    55.7 (+5.9)   44.9 (+.8.1)    8.2 (+5.9)

Napthalene             16.3 (+3.9)    11.9 (+1.2)   11.1 (+0.7)    3.4 (+1.6)

Dodecane               66.9(+_14.0)    66.0 (+6.5)   63.6 (+0.4)   35.0(+11.0)   0.5 (+_ .8)

Tridecane              56.0(+10.6)    60.7 (+6.4)   64.3 (+3.3)   48,4 (+8.1)  11.1 (+5.8)

Tetradecane            43.1 (^7.8)    49.8 (+4.7)   50.7 (j+4.6)   44.8 (+.6.7)  32.3 (+_6.1)

Pentadecane            16.4 (+2.7)    18.2 (+2.0)   32.7 (+2.2)   14.7 (+2.4)  19.3 (+_ .9)

Hexadecane	-	-	-     	-	-	-	

Concentrations (mg/£)a of selected  hydrocarbons in sterile water bottles from quiescent bottle test,
using water samples from  Escambia River and petroleum-derived JP-4.

aAverage of replicate samples.
bBad replicate; n=l
Parentheses indicate one  standard deviation from the mean.
Dashes (-) indicate not detectable  (<0.2 mg/Ji) .

-------
             TABLE  21.   DATA FROM ESCAMBIA RIVER BOTTLE  TEST,  STERILE SEDIMENT WITH PJP-4
Hydrocarbon
Benzene
Cycl ohexane
2,3-Dimethyl pentane
3-Methylhexane
Day 0 Day 1 Day 2 Day 4
13.2 (+_ 0)
48.5 (+0.5) ..-
71.4 (+1.3)
51.6 (+1.0) 25.4 (+0.6) 32.9 (+4.3)
Day 8C Day 13
-
-
-
-
Heptane               2310.0(+48.1)   270.5 (+_5.9) 326.8(+_28.0)  176.0(+39.1)



Methylcyclohexane       58.4 (+1.5)      -           1.0  (+0.1)



2,5-Dimethylhexane      16.8 (+0.3)      -



2,4-Dimethylhexane      28.2 (+0.8)



Methylbenzene           28.1 (+0.9)      -           0.6  (+0.2)



2-Methyl heptane         91.6 (+3.7)      -           2.6  (+0.0)    3.9 (+2.5)



3-Methylheptane        114.2 (+4.5)      -           3.5  (+_0.3)    5.1 (+_3.3)



1,1-Dlmethylcyclohexane 3.7 (+0.2)      -



Octane                 161.1 (+_6.9)     1.1 (+_0.6)   4.8  (+_0.7)    7.9 (+_4.8)



Ethyl cycl ohexane       40.0 (+1.8)      -           1.1  (+0.8)    1.0 (+_1.3)



Ethylbenzene           15.3 (+0.7)      -



rri-Xylene                28.6 (+_1.7)



2-Xylene                23.5 (+_0.8)      -            -            0.7 (+ .3)



o-Xylene                22.9 (+1.0)

-------
      TABLE 21.  DATA FROM ESCAMBIA RIVER BOTTLE TEST, STERILE SEDIMEN1  WITH PJP-4 (CONCLUDED).
Hydrocarbon
Nonane
Isopropyl benzene
1 , 3 ,5-Trimethyl benzene
1 , 2, 4-Trimethyl benzene
Decane
1,2, 3-Trimethyl benzene
Indan
Undecane
Naphthalene
Dodecane
Tridecane
Tetradecane
Pentadecane
Hexadecane
91.
2.
24.
31.
77.
14.
4.
83.
16.
72.
60.
43.
15.
_
Concentrations (mgA)a of
test, using sediment samp!
- 0
5 (±4.6)
5 (±0.4)
7 (±1.2)
9 (+1.4)
4 (±3.9)
6 (±0.6)
9 (±0.1)
5 (±3.6)
6 (±0.5)
3 (±2.6)
6 (±3.0)
1 (+ 0)
9 (±0.4)

selected
es from
Day 1
1.5
-
1.4
2.5
15.8
1.8
0.7
49.3
10.7
60.9
55.3
43.6
15.9
-
(±

(±0
(±0
(±2
(±0
(±0
(±3
(±0
(±2
(±2
(±1
(±0

0)

.3)
• 7)
.6)
.3)
.1)
.2)
•6)
.5)
.0)
.6)
.7)

hydrocarbons i
Escambia River
Day
3.
-
0.
1.
8.
0.
-
45.
11.
70.
69.
50.
21.
-
3 (±0.

8 (±0.
0 (±0.
1 (±5.
8 (±0.

3 (±20.
6 (±3.
2 (±24.
2(±24.
9(±15.
8 (±9.

n sterile
and
petrol
8)

7)
9)
0)
7)

6)
9)
4)
3)
8)
6)

Day
5.4
-
0.9
-
4.7
-
-
10.4
3.8
30.6
37.6
30.6
11.2
-
sediment
eum-deri
4_
(±3

(±

(±2


(±4
(±
(±5
(±5
(±3
(±

Day 8C Day 13
.1)
-
.5) -
-
.7)
-
-
.5)
1)
.9)
.4) 7.5
.5) 8.2
.9) 5.9
_ _
bottles from quiescent bottle
ved
JP-4.
aAverage of replicate samples.
bBad replicate; n=l
^Day 8 - No duplicate sample.
Parentheses indicate one standard deviation from the mean.
Dashes (-)  indicate not detectable (<0.2 mg/£).

-------
TABLE 22.  DATA FROM ESCAMBIA RIVER BOTTLE TEST, ACTIVE SEDIMENT WITH PJP-4
Hydrocarbon
Benzene
Cyclohexane
2,3-Dimethyl pentane
3-Methylhexane
Heptane
Methyl cyclohexane
2,5-Dimethylhexane
2,4-Dimethyl hexane
Methyl benzene
2-Methyl heptane
3-Methyl heptane
Day 0
13.2 (+0.1)
43.8 (+3.4)
65.3 (+_5.0)
48.1 (+3.2)
1874.3(+86.3)
56.1 (+2.3)
16.6 (+0.5)
27.7 (+0.7)
29.0 (+0.7)
92.1 (+_ 0)
113.1 (+0.2)
1,1-Dlmethyl cyclohexane 3.8 (+_ 0)
Octane
Ethyl cyclohexane
Ethyl benzene
m-Xyl ene
jD-Xylene
o-Xylene
165.2 (+4.1)
41.3 (+1.4)
16.0 (+0.7)
31.3 (+0.8)
23.2 (+3.5)
22.8 (+1.3)
Day 1 Day 2 Day 4 Day 8 Day 13
_
-----
3.1 (+4.5)
47.2(+56.3) - 13.2 (+_ .5)
41.3(+36.6) 318.3(+167.0) -
55.9(+_68.3) - - -
3.1 (+3.5)
_
8.3(^11.8)
2.3 (+2.2) 55.7(+_57.0) -
3.4 (+_3.3) 66.4(^63.0) - 0.7 (+_ 1)
0.8 (+1.1) -
5.1 (+_4.9) 187.6(+_178.2) - 1.1 (^1.5)
16.9(+17.0) -
9.0(+12.8)
6.2 (+8.8)
13.9(+16.1) -
9.4(+_13.3)

-------
                      TABLE 22.  DATA FROM  ESCAMBIA  RIVER  BOTTLE  TEST,  ACTIVE SEDIMENT WITH PJP-4 (CONCLUDED).


               Hydrocarbon            Day 0          Day 1         Day 2         Day 4        Day 8        Day 13

               Nonane                 96.2  (+_5.7)     4.7 (+0.3)   46.7(+43.3)     -           0.7 (+_  1)

               Isopropylbenzene        2.6  (+0.7)      -

               1,3,5-Trimethylbenzene 26.2  (+1.7)     6.7 (+2.7)    9.9 (+.9.4)

               1,2,4-Trimethylbenzene 34.9  (+2.3)     4.9 (+1.2)   20.0(^19.7)

               Decane                 83.9  (+_5.7)    23.3 (+.1.4)   28.7(^14.6)     -           0.7 (+_  1)

               1,2,3-Trimethylbenzene 15.7  (+1.1)     3.1 (+0.6)    3.8 (+.3.1)

               Indan                   5.2  (^0.5)     1.0 (+.0.1)    1.9 (^1.8)

^              Undecane               90.3  (+6.2)    57.1 (+4.5)   32.8 (+4.7)   14.7 (+3.8)    1.0 (+1.5)
PO
               Napthalene             17.5  (+1.0)    12.6 (+.1.1)    8.6 (+0.7)    4.7 (+_ .2)

               Dodecane               78.4  (+5.1)    70.1 (+.7.6)   35.4(+_13.5)   41.4 (+3.9)    1.4(+1.2)

               Tridecane              65.8  (+3.8)    59.5 (+6.8)   28.7(+_13.9)   44.9 (^2.8)    7.8 (+4.7)

               Tetradecane            47.4  (+4.0)    48.0 (+6.0)   19.4(^13.0)   36.0 (+.1.8)   20.1 (+.5.8)

               Pentadecane            16.7  (+1.1)    18.7 (+2.5)    6.3 (+4.4)   12.9 (+_ .6)   10.3 (+1.5)

               Hexadecane	-	-	-	-	-	-	

               Concentrations (mgA)a of selected hydrocarbons  in  active sediment bottles from quiescent bottle test,
               using sediment samples from Escambia  River  and Petroleum-derived JP-4.

               aAverage of replicate samples.
               t>Bad replicate; n=l
               Parentheses indicate one standard deviation from the mean.
               Dashes (-)  indicate not detectable (<0.2 mg/a).

-------
                            TABLE  23.   COMPARISON  OF  DEGRADATION RATES IN THE ESCAMBIA RIVER TEST
--J
CO
Sterile
Hydrocarbon
Undecane
Ethyl cyclohexane
Decane
Decane
j
>
Hydrocarbon
Decane
Decane
Nonane
Undecane
Source
Shale
Shale
Petroleum
Shale
Sample
Steril
Active
Active
Active
Sample
Type
Sediment
Sediment
Water
Sediment
Type
e water
water
sediment
sediment
Confidence
Rate(h~!) Limits
-.0069
-.011
-.0233
-.0116
Shal
+.0056
+ .005
+.0188
+.0006
e-de rived
to -
to -
to -
to -
.008
.0168
.0276
.0224
Active
Confidence
RatesCh'1) Limits
-.0086
-.0276
-.0262
-.0096
+.0062
+.1019
+.0104
+.054
to -
to -
to -
to -
.0108
.157
.0627
.0731
Significant
Difference
None
None
None
None
Petroleum derived
Confidence
Rate(h'l) Limits
-.0208
-.0216
-.0261
-.0086
+.0164
+.0159
+.0674
+.0062
to -
to -
to -
to -
.025
.0271
.1195
.0108
Rates(
-.0233
-.0262
-.0087
-.0100
Confidence
h'1) Limits
+.0188
+.0104
+.045
+.0075
to -
to -
to -
to -
.0276
.0627
.0623
.0123
Significant
Di f ference
None
None
None
None
 Comparison of  rates  of  disappearance  of  selected  hydrocarbons  from  quiescent  bottle
 tests containing water  and  sediment from Escambia  River  relative  to sterile and  active  systems
 (top) and fuel types  (bottom).

-------
   DPM(XIOOO)
100
 75
 50
 25
  0
                                      \
                                      \
        BOTTLE CONTROL
SEAWATER CONTROL
SJP4 EXPOSED
         Figure 17.  Decane Mineralization Following Range Point Test
                                   74

-------
                            C02
                    WATER
                      ...
                   U. - - >.	v _-^	J
600000
      DPM
 ORIGINAL SPIKE = 1 X 10(
400000 -
200000»-
             SJP-4
SJP-4 and
FORMAUN
TOLUENE
                                 PRE-EXPOSURE
                                    SUBSTRATE
            Figure  18.  Toluene Toxiclty In Range  Point Water
NONE
                                  75

-------
be variable.  Gas chromatographic analysis of the fuel  remaining at each



sampling time indicated enrichment of high boiling hydrocarbons as the



test progressed.  Gas chromatographic analysis of jet  fuel  from the day-2



sample indicated that all  the aromatics  were below detection  limits; the



remaining fuel  was composed entirely of  aliphatic hydrocarbons.
                                    76

-------
                    STERILE

                    24 HOURS
                                 ACTIVE

                               24 HOURS
 SRERILE

48 HOURS
 ACTIVE

48 HOURS
       20
LU
 .
O
^
LL
O
z
o

t?

-------
LJJ
Z
LU
NJ
Z
LLJ
CD
X

LLJ
2
cc
       15
       10

LL
O
Z
O

<
cc
LU
O
z
O
O
                     STERILE
                    24 HOURS
 ACTIVE
24 HOURS
 STERILE
48 HOURS
 ACTIVE
48 HOURS
              NATURAL WATER
                                 1,3,5-TRIMETHYLBENZENE
    +400 MG/L DOC
              +800 MG/L DOC
                          DISSOLVED ORGANIC CARBON
      Figure 20.   Solubility  of 1,3,5-Trimethylbenzene  Versus DOC
                                78

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100
 90
 80
 70
 60
 50
 40
 30
 20
 10
  0
   0    10   20   30   40   50   60   70   80   90   100  110  120  130  140  150
                                         Time
                                         Hours
                   Figure 21.  Jet Fuel Evaporation Rate
                                     79

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                                Section IV




                                CONCLUSIONS





     Little difference was found between shale-derived JP-4 and petroleum-



derived JP-4.  Under virtually all  conditions tested,  volatility was the



overwhelming determining factor in  the fate  of the component hydrocarbons.



The physical similarity of the two  fuels,  as seen  in the compositional



analysis, precludes the possibility of detecting  any differences under



these test conditions.   Coupled with the importance of volatility,  this



indicates that there would be little difference in the fates of the two



fuels under most environmental  conditions.



     The similarity of the fuels extends to  the water-soluble fractions



derived from PJP-4 and SJP-4.  Except for  one hydrocarbon component,



benzene, the water-soluble fractions, which  cause  environmental  damage  if



a spill occurs, are essentially identical.



     The results from the quiescent bottle tests  suggest that volatility



is the principal loss mechanism of  the hydrocarbons in shale-derived jet



fuel  from water but (Range Point water)  biodegradation is sometimes



important.  In fact, we believe that biodegradation will only be detected



in the quiescent bottle test if the hydrocarbons  are relatively slow to



evaporate; i.e., the lack of any detectable  biodegradation of SJP-4 in



samples from two of the three sampling sites, was  largely because hydro-



carbons were lost so rapidly by evaporation.  The  apparent absence of



biodegradation of SJP-4 hydrocarbons at these sites, differs somewhat



from the results of tests with PJP-4, where  some  biodegradation of certain



hydrocarbons in water samples from  Escambia  River  was  apparent.  It is



possible that the difference in results was  because SJP-4 was more volatile



than PJP-4 and thus no biodegradation was detected.  Despite the large



                                    80

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part played by volatilization, mineralization studies using 14C-labeled
hydrocarbons indicated that biodegradation probably was occurring and
thus^played a role in removal of JP-4 hydrocarbons.  Circumstances that
reduce volatility, such as increased hydrocarbon solubility as a function
of water chemistry, would make the role of microbial degradation more
important.
     The unusually high number of hydrocarbons that degraded in the quie-
scent bottle tests containing water samples from Range Point was probably
due to either an artifact in the biodegradation test procedure or a unique
environmental factor associated with the Range Point water rather than to
the hydrocarbon compostion of the SJP-4.  An attempt was made to distinguish
between the two possibilities.  Disappearance rates for 10 selected hydro-
carbons, cyclohexane, ethylbenzene, £-Xylene, 1,2,4-Trimethylbenzene, decane,
undecane, naphthalene, dodecane, tridecane and tetradecane, in quiescent
bottle experiments with SJP-4 and PJP-4 were calculated (Tables 24 and 25).
Confidence intervals calculated from the slopes of semilog plots indicate
that, in most cases, differences in rates between sterile and active systems
with each experiment were significantly different (confidence intervals do
not overlap).
     Comparison of results with SJP-4 to results from previous studies with
PJP-4 and samples from Range Point salt marsh showed that biodegradation
rates of the indicated hydrocarbons were probably the same, regardless of
the fuel source (Table 26).  This was determined by subtracting the rate
of disappearance of each hydrocarbon in the sterile water tests from its
disappearance rate in the active water test (i.e., separating out the true
biotic component).  What appears to be the difference between active and
sterile systems in the SJP-4 experiment is due largely to a lower volatility

                                    81

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                     TABLE 24.   RATE OF  DISAPPEARANCE OF  SELECTED  SJP-4  HYDROCARBONS  IN RANGE POINT TEST
CO
ro
Hydrocarbon
Cyclohexane
Ethyl benzene
_p_-Xylene
1,2,4-Trimethyl-
benzene
Decane
Undecane
Napthalene
Dodecane
Tridecane
Tetradecane

Rate
-.024
-.002
-.002
-.004
-.001
-.0015
-.0004
-.0007
-.0008
-.0006
Sterile

Confidence Limits3
+.098 to
-.0004 to
-.001 to
-.0015 to
+.0002 to
+.0001 to
+.0001 to
Od to
-.0002 to
Od to
-.146
-.003
-.0025
-.0051
-.0009
-.001
-.0008
-.0012
-.0012
-.001
Rate
	 C
	 C
	 c
-.017
-.009
-.005
-.005
-.005
-.004
-.003
Confidence Limits3


+ .005
-.0052
-.0021
-.003
-.0035
-.0026
-.0013


to
to
to
to
to
to
to


-.035
-.0134
-.0067
-.0056
-.0067
-.005
-.0039
Significant
difference*3


Yes
Yes
Yes
Yes
Yes
Yes
Yes
        Rates  of disappearance  of selected  hydrocarbons  in  shale-derived jet fuel from quiescent bottle tests containing
        water  from range  point  salt  marsh.
        ^Confidence intervals  do  not  overlap.
        ^Hydrocarbons  not  detected  after t=o sampling.
        dlnsufficient  data points to  calculate  complete  confidence  limits.

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                    TABLE 25.  RATE OF DISAPPEARANCE OF SELECTED PJP-4 HYDROCARBONS  IN RANGE POINT TEST
oo
GO
Hydrocarbon
Cyclohexane
Ethyl benzene
£-Xylene
1,2,4-Trimethyl-
benzene
Decane
Undecane
Napthalene
Dodecane
Tridecane
Tetradecane

Rate
-.324
-.008
-.005
-.009
-.010
-.009
-.008
-.006
-.003
-.002
Sterile


Confidence Limits'5
+.9694
-.0021
-.0096
-.0045
-.0055
-.007
-.005
-.004
-.0016
-.0008
to
to
to
to
to
to
to
to
to
to
-1.6163
-.0125
-.100
-.0133
-.0135
-.0106
-.010
-.0072
-.004
-.0028
Rate
	 d
-.163
-.063
-.051
-.021
-.023
-.016
-.011
-.007
-.004
Confidence Limits'5

-.0903
-.0185
-.0428
-.0154
-.0174
-.0143
-.0093
-.005
-.0024

to
to
to
to
to
to
to
to
to

-.2343
-.1061
-.0592
-.0268
-.0290
-.0179
-.0119
-.0092
-.0054
Significant
difference0

Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
       Rates of disappearance of selected hydrocarbons in petroleum-derived jet fuel  from quiescent bottle tests
       containing water from Range Point salt marsh3

       aSource:  Spain, J.C., C.C. Somerville, T.J. Lee, L.C. Butler, A.W. Bourquin,  "Degradation Jet  Fuel
        Hydrocarbons by Aquatic Microbial Communities," interim report, 23 October, 1981 to 30 September 1982,
        pp. 182-185.

       t> a=0.05

       cConfidence  intervals do not overlap.

       ^Hydrocarbons not detected after t=o sampling.

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     TABLE 26.  COMPARISON OF BIOTIC DEGRADATION RATES IN RANGE POINT TEST
Hydrocarbon
Cyclohexane
Ethyl benzene
_p_-Xylene
1,2,4-Trimethyl-
benzene
Decane
Undecane
Napthalene
Dodecane
Tridecane
Tetradecane
Active
SJP-4
-
-.155
-.058
-.042
-.011
-.014
-.008
-.005
-.004
-.002
Water3
PJP-4
-
-
-
-.013
-.008
-.0035
-.0046
-.0043
-.0032
-.0024
PJP-4/SJP-4
-
-
-
.31
.73
.25
.58
.86
.80
1.2
Comparison of biotlc rates of hydrocarbon disappearance from quiescent bottle
tests containing either shale-derived (SJP-4)  or petroleum derived (PJP-4)  jet
fuel  and water samples from Range Point salt marsh.

aActive water rates corrected for losses due to volatilization (sterile water)
                                      84

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of hydrocarbons in this test than in the previous PJP-4 experiment
(Table 27).  Previously, then, if volatility had been reduced in the
PJP-4 experiment, we would have seen a similar contribution of the biotic
component.  These results are important relative to the fate of jet fuels
in the environment because under conditions in which volatilization might
be restricted, for whatever reasons, biodegradation appeared sufficient
to maintain at least some continued loss of the hydrocarbons from the
environment.
     The difference in volatility rates between the two experiments could
be the result of differences in fuel composition.  For example, unidentified
volatile hydrocarbons present in the SJP-4, but not in the PJP-4 may have
saturated the head space in the bottles and,thereby, reduced volatility.
However, it is more likely that experimental variability caused by such
factors as differences in temperature, air  flow into and out of the bottles
and even sampling schedules, had the major  impact on volatility.
     The slower volatility rates may also be of environmental significance
because the underlying mechanism may shed light on factors that control
hydrocarbon residence time in the affected  environment.  Although, air move-
ment in and out of the bottle was not tightly controlled, we do not believe
that laboratory conditions during the incubation period were responsible
for the slower volatility; repeating the test, for example, with aluminum
foil  closures to restrict evaporation losses did not result in an increased
amount of biodegradation.  These results ruled out the possibility of an
artifact in the fate test system.
     The addition of inorganic nutrients to the test waters, did not affect
biodegradation rates.   Under the assumption that Range Point water may have
had higher concentrations of dissolved organic carbon (DOC), a condition
                                    85

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  TABLE 27.  COMPARISON OF ABIOTIC DEGRADATION RATES IN RANGE POINT TEST
Hydrocarbon
Cyclohexane
Ethyl benzene
£-Xylene
1,2,4-Trimethyl-
benzene
Decane
Undecane
Naphthalene
Dodecane
Trldecane
Tetradecane
Sterile
SJP-4
-.024
-.002
-.002
-.004
-.001
-.0015
-.004
-.0007
-.0008
-.0006
Water
PJP-4
-.324
-.008
-.005
-.009
-.010
-.009
-.008
-.006
-.003
-.002
PJP-4/SJP-4
14.2
4
2.5
2.1
10.0
6.1
20.0
8.5
3.5
3.3
Comparison of abiotic rates of hydrocarbon disappearance from quiescent
bottle tests containing either shale-derived (SJP-4)  or petroleum-derived
(PJP-4)  jet fuel  and water samples from range point salt marsh.
                                    86

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that we and others (Reference 6) have shown will increase the solubility of
the hydrocarbons and decrease their volatility, a degradation test was per-
formed using a humic acid preparation from sediment to artificially increase
the DOC.  Biodegradation in the test was increased by the presence of the
additional DOC but the concentration of the DOC required was unrealistically
high (Figures 19, 20).  The effect we observed, however, was roughly linear
and consequently the effect of  DOC we observed was probably operational at
environmentally realistic DOC levels (Figures 19,20).  DOC concentration in
environmental samples should be checked because it could reduce losses of
spilled jet fuel by volatilization.
     Finally, certain other circumstances also present the possibility of
increased environmental risk.   According to the results of our quiescent
bottle tests, fuel hydrocarbons may strongly sorb to sediments and remain
in the receiving environment for longer periods.  This result was also
observed in previous PJP-4 studies.  If these hydrocarbon carrying sediments
fall into the anoxic areas of a body of water, they may represent a signifi-
cant sink of potentially damaging  hydrocarbons  (Reference 7).
                                    87

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                                Section V



                             RECOMMENDATIONS





     Our test results indicated that SJP-4 and PJP-4 should be treated in a



similar fashion in the event of a spill.   Most small-scale spills require



little treatment other than those precautions normally taken for safety



reasons.  In larger spills containment and recovery operations would prob-



ably be necessary.  Other than those two  general  guidelines, specific



recommendations are not possible with our present data base, either as to



SJP-4 versus PJP-4 or to jet fuels in general.  Our investigations indicate



that a variety of environmental factors can and do effect the fate of jet



fuels in aquatic environments.  A spill  in a placid, pristine marsh may



result in a drastically different situation than  a similar spill  in an



actively flowing, heavily impacted river.  Recommendations for one situ-



ation could prove disastrous in the other.



     Further research is indicated in four areas: (1)  the fate of hydro-



carbons sorbed* to particulates especially in terms of oxygen availability;



(2)  the role of water chemistry in the solubility/fate of hydrocarbons; (3)



toxicity of the water soluble fraction of fuels to representative aquatic



species as a function of time and concentration;  (4) toxicity of the WSF



to the resident microbial  population and  the ability of the bacteria to



recover from this effect (i.e., determine the toxic threshold concentration



under different environmental  conditions); (5)  an investigation into the



causes of the variability in test results from site to site.  Our data indi-



cate that parameters we do not as yet understand  have a significant impact



on the fate of jet fuels in aquatic environments.  Environmental  factors



such as dissolved organic carbon, dissolved oxygen, pH, salinity, etc.,
                                    88

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are all potential determining factors in the ultimate fate of jet  fuels
in aquatic systems.  Until the effect (or lack of it)  of these parameters
on the fate of jet fuels is understood, it will be difficult, if not
impossible to make any valid site-specific predictions about the outcome
of a fuel spill of any proportion.
                                     89

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                                REFERENCE


1.  Ghassemi, M., A. Panahloo and Oulivan, S., "Comparison of Physical
    and Chemical  Characteristics of Shale Oil  Fuels and Analogous Petroleum
    Products," Environmental  Toxicology and Chemistry, vol 3, pp. 511-535.
    1984.

2.  Hayes, P.C, and Pitzer, E.W., Characterizing Petroleum- and Shale-
    Derived Jet Fuel Distillates via Temperature-programmed Kovats Indices.
    Chromatography, vol. 253, pp. 179-198, 1982.

3.  Hunt, T.P., Standard procedure for preparing saturated water soluble
    fractions of jet fuels.  Unpublished report, Environmental  Quality Branch,
    Toxic Hazards Division, Air Force Aerospace Medical Research Laboratory,
    Wright-Patterson AFB, Ohio  45433.

4.  Spain, J.C.,  Somerville,  C.C., Lee, T.J.,  Butler,  L.C., and Bourquln,
    A.W., Degradation of Jet  Fuel Hydrocarbons by Aquatic Microbial  Communities,
    EPA-600/X-83-059, U.S. Environmental  Protection Agency, Gulf Breeze, FL, 1983.

5.  Lake, J.L., Dimock, C.W.  and Norwood, C.B., A Comparison of Methods for the
    Analysis of Hydrocarbons  in Marine Sediments.  Advances in  Chemistry Series,
    #185, L. Petrakes and F.T. Weiss (eds.)  Petroleum  In the Marine  Environment,
    1980.

6.  Boehm, P.O. and Quinn, J.G., "A Chemical  Investigation of the Transport
    and Fate of Petroleum Hydrocarbons in Littoral  and Benthic  Environments
    of the Tsesis Oil Spill," vol. 6, pp. 157-173,  1982.

7.  Pritchard, P.H., Mueller, L.H,. Spain, J.C. and Bourquin, A.W.,  Degradation
    of Jet and Missle Fuels by Aquatic Microbial  Communities, Report to the Air
    Force, Interagency Agreement No. AR-57-F-2-A-016,  1986.
                                    90

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