PB98-963144
                              EPA 541-R98-156
                              March 1999
EPA Superfund
      Record of Decision Amendment:
      Allied Chemical & Ironton Coke
      Ironton, OH
      9/30/1998

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                     RECORD OF DECISION AMENDMENT #3
             ALLIED CHEMICAL/IRONTON COKE SUPERFUND SITE
                                    Ironton, Ohio
PURPOSE
This decision document, together with the Allied Chemical/Ironton Coke Record of Decision
(ROD) dated December 28, 1990, the first Allied Chemical/Ironton Coke ROD Amendment
dated July 31, 1995 (ROD Amendment #1), and the second ROD Amendment dated September
4, 1997 (ROD Amendment #2), presents the selected remedial action for the Allied
Chemical/Ironton Coke site. The cleanup remedy for the site has been developed in accordance
with the Comprehensive Environmental Response, Compensation and Liability Act of 1980
(CERCLA), as amended by the Superfund Amendments and Reauthorization Act of 1986
(SARA), and, to the extent practicable, the National Oil and Hazardous Substances Pollution
Contingency Plan (NCP) and Agency Policy.

It is anticipated that the State of Ohio will concur with this decision.  A written confirmation is
expected and will be added to the administrative record upon receipt.

BASIS

The decision to further amend the Allied Chemical/Ironton Coke ROD and ROD Amendments
and select a modified remedial action is based upon the Administrative Record. The attached
index lists the items that comprise the Administrative Record for ROD Amendment #3.

ASSESSMENT OF THE SITE

Actual or threatened releases of hazardous substances from this site, if not addressed by
implementing the response actions selected in the ROD, ROD Amendments #1 and #2, and ROD
Amendment #3, may present an imminent and substantial endangerment to public health,
welfare, or the environment.

DESCRIPTION OF THE REMEDY

The remedy selected in the 1990 ROD, 1995 ROD Amendment #1, and 1997 ROD Amendment
#2 for the site is a final remedial action. The major components of the selected remedy include:

•      Incineration of approximately 122,000 cubic yards of lagoon waste materials and on-site
       re-use of the waste heat generated during incineration.

•      In-situ bioremediation of approximately 457,000 cubic yards of contaminated soil
       materials.

       Off-site disposal of approximately 40,000 cubic yards of contaminated soil material
       referenced as the "ROD Soils."

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                                          2

       Pumping and on-site treatment of groundwater.

•      Downgradient groundwater monitoring of Ice Creek and preparation of a contingency
       plan. Implementation of deed restrictions, fencing and security.

Through ROD Amendment #3 the following components of the selected remedy are being
modified:

•      Replace in-situ bioremediation of 457,000 cubic yards of soil in Lagoons 1-4 with hot
       spot excavation and wetland development.
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       Replace incineration of Lagoon 5 materials with recycling, treatment, and/or disposal of
       the KO87 listed waste in an approved off-site hazardous waste facility and the use of the
       remaining material, excluding debris, as an alternative fuel.

STATUTORY DETERMINATIONS

The selected remedy is protective of human health and the environment, complies with federal
and state requirements that are legally applicable or relevant and appropriate to the remedial
action, and is cost-effective. Hot spot excavation and wetland development of the 457,000 cubic
yards of soil in Lagoons 1-4 only partially meets the requirement of reduction of toxicity,
mobility, or volume through treatment. Since the soils in Lagoons 1-4 are not as contaminated as
previously thought and hot spot excavation can achieve an alternate clean-up level  proposed in
the original ROD, as well as the beneficial contribution of wetland development to valuable
ecological habitat, these changes are justified. However, the use of recycling, treatment and/or
disposal of the Lagoon 5 materials does satisfy the statutory preference for treatment as a
principal element of the  remedy and employs permanent solutions and alternate treatment
technologies to the maximum extent possible.

The remedial action selected in the ROD and by ROD Amendments #1, #2, and #3 will  result in
a hazardous substance remaining on-site above health-based levels.  Therefore, a "Five-Year
Review" will be conducted after commencement of the remedial action and every five years
thereafter to ensure that  the remedy continues to provide protection of human health and the
environment.
William E. Muno, Director/                              '          Date
Superfund Division

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                                         1

                     RECORD OF DECISION AMENDMENT #3
             ALLIED CHEMICAL/IRONTON COKE SUPERFUND SITE

I.      INTRODUCTION

The Allied Chemical/Ironton Coke Superfund Site, located in Ironton, Lawrence County, Ohio is
approximately 95 acres in size. The site consists of a dismantled Coke Plant which operated
from 1920 to 1982 and five lagoons which received process wastewater and hazardous solid
waste from the former Coke Plant. Figure 1 is a map of the Coke Plant and Lagoon areas.  A 4-
acre waste pit called the Goldcamp Disposal Area (GDA) is also part of the site and an operating
AlliedSignal Tar Plant is within the site boundaries. The Allied Chemical/Ironton Coke site is
divided into two operable units, the GDA and the Coke Plant/Lagoon Area (CPLA).

The GDA Record of Decision (ROD) which describes the GDA site remedy was executed on
September 29, 1988.  The remedial design/remedial action (RD/RA) for the GDA is being
implemented through a Comprehensive Environmental Response, Compensation, and Liability
Act of 1980 (CERCLA), as amended, Section 106 Unilateral Administrative Order. The
Unilateral Administrative Order (UAO) was issued to AlliedSignal, Inc. and Amcast Industrial
Corporation on March 9,1989. AlliedSignal has complied with the UAO.

The CPLA RD/RA is also being performed through a CERCLA Section 106 UAO which was
signed on July 1, 1991, and was issued to AlliedSignal, Inc. The CPLA remedy was finalized
through the ROD signed on December 28,1990, and subsequently amended on July 31, 1995
and September 4,  1997.

Pursuant to CERCLA Section 117 and the National Contingency Plan (NCP), Section
300.435(c)(2)(I), the United States Environmental Protection Agency (U.S. EPA) is publishing
this ROD Amendment. The ROD Amendment by the U.S. EPA is a result of new information
discovered during the RD/RA for the CPLA operable unit. This ROD Amendment describes a
fundamental change to the CPLA ROD.  A Proposed Plan  was published on December 1, 1997,
followed by a 30 day public comment period which ended on January 2, 1998. Only public
comments  in support of the proposed plan were received during the public comment period. This
ROD Amendment will become part of the Allied Chemical/Ironton Coke Administrative Record
(NCP 30.825(a)(2)), which is available for review at the Briggs Lawrence County Library,
located in Ironton, Ohio. The information used in U.S. EPA's assessment of this change is
currently available at the above repository.

II.     REASONS FOR ISSUING THE ROD AMENDMENT

The remedy as described in the original ROD for the CPLA operable unit  contained the
following components:

•      Incineration of approximately 122,000 cubic yards of lagoon waste materials and on-site

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       re-use of the waste heat generated during incineration, referenced as Lagoon 5 soils;

•      In-situ bioremediation of approximately 475,000 cubic yards of contaminated soil
       materials, referenced as Lagoon 1-4 soils;

•      Prepared pad surface bioremediation of approximately 40,000 cubic yards of
       contaminated soil material, referenced as the "ROD Soils";

•      Pumping and on-site treatment of groundwater; and

•      Downgradient groundwater monitoring of Ice Creek a/id preparation of a contingency
       plan. Implementation of deed restrictions, fencing, and security.

Based upon new information discovered during the pre-design and design for the CPLA operable
unit, the 1995 ROD Amendment #1 made four changes to the 1990 ROD and they are as follows:

•      Removal of the waste heat boiler from the incineration process for Lagoon 5;

•      Removal of the dismantlement provision for the incinerator;

•      Excavate and store on-site for eventual treatment or placement into the lagoon area,
       135,000 cubic yards of soils referenced as the "Site Soils"; and

•      Revise the cleanup standard for groundwater constituents benzo(a)pyrene and
       dibenz(a,h)anthracene at the GDA and CPLA from a total of 5 parts per trillion (ppt) to
       safe drinking water standards of 200 ppt for benzo(a)pyrene and 300 ppt for
       dibenz(a,h)anthracene.

Additional sampling and analysis for a group of soils classified as the ROD Soils determined that
carcinogenic polynuclear aromatic hydrocarbons (PAHC) within the ROD Soils was not as high
as previously thought. The lower level of PAHC allowed the agency to revisit the remedy for the
ROD Soils. This resulted in the 1997 ROD Amendment #2 which made  a single change to the
1990 ROD for the CPLA operable unit that is as follows:

•      Replacing prepared pad bioremediation of the approximately 40,000 cubic yards of ROD
       Soils with off-site disposal in an approved landfill.

ROD Amendment #3 addresses requests from AlliedSignal that the U.S.  EPA revise and replace
the treatment of 457,000 cubic yards of Lagoon 1-4 soils from in-situ bioremediation to hot spot
excavation and wetland development and revise the treatment of 122,000 cubic yards of Lagoon
5 soils from incineration to containment. While U.S. EPA does not believe containment of
Lagoon 5 is appropriate, U.S. EPA does believe that modifying the requirement to incinerate
Lagoon 5 is appropriate.

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In the 1990 ROD for the CPLA operable unit Lagoons 1 -4 soils were required to be treated by in-
situ bioremediation. Through bioremediation, naturally occurring microorganisms are used to
break down the contaminants to levels which are protective of public health and the environment.
Water fortified with oxygen and nutrients is distributed throughout the lagoons to accelerate the
growth of the microorganisms.  During the design phase for the in-situ bioremediation, sampling
demonstrated that levels of PAHC compounds were not as high as previously thought. In
addition, several pilot tests indicated that achieving the 0.97 parts per million (ppm) cleanup
standard established in the 1990 ROD through in-situ bioremediation would be difficult.  This
proposed change is based upon using the alternative wetland cleanup standard that is provided in
the 1990 ROD for the CPLA operable unit. The CPLA ROD states that the cleanup standard for
soil is 0.97 ppm for PAHC. This standard was based on a direct contact exposure pathway and
assumed residential land use.  An alternative cleanup standard of 97 ppm for PAHC was
provided in the CPLA ROD. The CPLA ROD provided for utilization of the 97 ppm PAHC
cleanup standard if the in-situ bioremediation would not achieve the 0.97 ppm clean-up standard
in a timely manner  and the threat of direct contact from lagoon soils through residential land use
was eliminated by flooding Lagoons 1-4 to create a wetland.  An assessment of the Lagoon 1-4
area indicates that the area is more likely to be an ecological area then a residential area in the.
future due to its close proximity to Ice Creek and the fact that this low-lying area has
historically served as a flood water storage area.  AlliedSignal requested that the U.S. EPA allow
utilization of the alternative cleanup standard of 97 ppm for PAHj prior to development of the
wetland. Based upon a review of the sampling data gathered from Lagoons 1-4 during design
and the unlikelihood that in-situ bioremediation would achieve the .97 ppm cleanup standard for
PAHC, the U.S. EPA evaluated two options for the Lagoon 1-4 soils:

•       In-situ bioremediation (the original selected remedy); and

•       Excavation of materials above 97 ppm PAH,, ("hot spot excavation") and subsequent
       wetland development.

The 1990 ROD for  the CPLA operable unit required incineration of approximately 122,000 cubic
yards of wastes from Lagoon 5.  In addition, an estimated 8,800 cubic yards of tarry soils
excavated from near the former coke plant and placed on top of Lagoon 5 were to be incinerated.
Based on studies during the design it was determined that Lagoon 5 contains a soft tar; a hard tar;
coal/coke fines and debris. The soil boring data indicated that the soft tar, which is a listed
hazardous waste (KO87) and considered by the U.S. EPA to be a principal threat at the site, was
physically distinguishable from the hard tar and coal/coke fines, and was located within a
discrete area of Lagoon 5. This indicates that the material in Lagoon 5 could be separated during
excavation. Based  upon the soil boring data and the fact that  the remedy for Lagoon 5 had not
yet been implemented, the U.S.  EPA decided to review the remedy and proposed four options for
evaluation.  The four options included:

1.     On-site incineration of Lagoon 5 and the tarry soils (the original selected remedy);

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2.     Construction of a RCRA Subtitle C containment cell in Lagoon 2 for the 122,000 cubic
       yards of material in Lagoon 5 and the tarry soils;

3.     Recycle back to coke plants the soft tar, which is classified as KO87, with the remaining
       coal/coke fines and hard tar in Lagoon 5 being used as an alternative fuel. If it appears
       that the capacity is not available at coke plants to recycle the KO87, treatment and/or
       disposal of the material off-site in an  approved hazardous waste facility might be
       necessary. The 8;800 cubic yards of tarry soils on top of Lagoon 5 will be separated by
       screening into three types of material (tar, debris, and product for use in cement kilns).
       The tar will be used as an alternative  fuel. The debris, which consists of clean brick and
       concrete, will be placed back on-site into the excavated Lagoon 5.  Additional product
       from the tarry soils will be sent to cement kilns for use in their processes; and

4.     Recycle back to coke plants the soft tar (K.O87) and cap the remaining material in
       Lagoon 5.

III.    EVALUATION OF THE ALTERNATIVES

The Administrative Record, located at the Briggs Lawrence County Library, is available for
review and contains the information which was used to evaluate the alternatives. In the National
Contingency Plan (NCP), 40 CFR Part 300.430, the U.S. EPA has established nine criteria that
assist in determining the most appropriate remedial alternative to be selected for a site. The
criteria are designed  to select a remedy that will be protective of human health and the
environment, attain Applicable or Relevant and Appropriate Requirements (ARARs), utilize
permanent solutions  and treatment technologies to the maximum extent practicable, and be cost
effective.  The relative performance of the proposed fundamental changes mentioned above has
been evaluated using the nine criteria set forth in the NCP as the basis of comparison. These
nine criteria are summarized below:

Threshold Criteria
The selected remedy must meet the following threshold criteria:

1.     Overall Protection of Human Health and the Environment  addresses whether a
       remedy provides adequate protection and describes how risks are eliminated, reduced or
       controlled through treatment, engineering controls or institutional controls.
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2.     Compliance with Applicable or Relevant and Appropriate Requirements (ARARsl
       addresses whether a remedy will attain applicable or relevant and appropriate
       requirements under federal environmental laws and state environmental or facility siting
       laws or provide grounds for issuing a waiver.

Primary Balancing Criteria
The balancing criteria are used to compare the effectiveness of the remedies.

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3.     Long-term Effectiveness and Permanence refers to the amount of risk to maintain
       reliable protection of human health and the environment over time once cleanup goals
       have been met.

4.     Reduction of Toxicitv. Mobility or Volume Through Treatment is the anticipated
       performance of treatment technologies that may be employed in a remedy to reduce the
       harmful effects of principal contaminants, their ability to move in the environment, and
       the amount of contamination present.

5.     Short-term Effectiveness refers to the speed with which the remedy achieves protection,
       as well as the remedy's potential to create adverse impacts on human health and the
       environment during the construction and implementation period.

6.     Implementability is the technical and administrative feasibility of a remedy, including
       the availability of materials and services needed to implement the chosen solution.

7.     Cost addresses the estimated capital and operation and maintenance (O&M) costs,
       evaluated as the present worth cost. Present worth is the present value of the capital and
       future O&M costs of an alternative based on the time value of money.

Modifying Criteria
These criteria deal with support agency and community response to the alternatives.

8.     State Acceptance indicates whether, based on its review of the FS, the previous ROD
       and ROD amendments, and the Proposed Plan, the support agency (in this case, the
       OEPA) concurs with, opposes, or has no comment on the recommended alternative.

9.     Community Acceptance is assessed in the Record of Decision based  upon a review of
       the public comments received on the FS report, the previous ROD and ROD
       amendments, and the Proposed Plan.

The nine criteria were used to evaluate and compare the options for the remediation of Lagoons
1-4 and Lagoon 5.
EVALUATION OF REMEDY FOR LAGOONS 1-4

The two options considered for remediation of Lagoons 1-4 were:

       In-situ bioremediation; and

•      Excavation of materials above 97 ppm-PAHc ("hot spot excavation") and subsequent
       wetland development.

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Threshold Criteria

1.     Overall Protection of Human Health and the Environment

Both options are protective of human health and the environment. If in-situ bioremediation can
achieve the original .97 or the alternative 97 ppm PAHC cleanup standard it is protective.  Hot
spot excavation of approximately 6,800 cubic yards of material in Lagoons 1-4 will achieve the
alternative cleanup standard of 97 ppm as described in the 1990 ROD for the CPLA operable
unit. In addition, wetland development as part of the excavation option will contribute to
valuable ecological habitat, while continuing ecological studies will over time demonstrate
protection to ecological receptors. The 97 ppm cleanup standard will also result in residual risks
within U.S. EPA's acceptable risk range (IXIO'MXIO"6) based on a direct contact exposure to a
future resident, even though this type of land use is not reasonably anticipated in the future.

2.     Compliance  with Applicable or Relevant and Appropriate Requirements (ARARs)

Compliance with applicable or relevant and appropriate requirements (ARARs) must be met for
each option.  The original selected remedy, as described in the 1990 ROD for the CPLA operable
unit, component of in-situ bioremediation, complied with all ARARs, except for those that
required waivers. ARARs requiring waivers for the in-situ bioremediation, are listed in the 1990
ROD and include:

•       OAC 3745-57-03, Landfill Design and Operating Requirements. For in-situ
       bioremediation leaving hazardous waste in place, does not specifically meet the
       requirements of this rule; and

       OAC 3745-54-18, Location for Hazardous Waste Facilities.  In-situ bioremediation
       involves leaving hazardous waste on-site in areas that do not meet Ohio's siting
       requirements.

For the hot spot excavation/wetland development option off-site treatment or disposal in a
landfill would require compliance with the State's regulatory equivalent of RCRA 40 CFR Part
261, Toxicity Characteristics. Toxicity characteristic leaching potential (TCLP) testing and
analysis will help determine the off-site treatment or disposal destination of the excavated soils.
Ohio Revised Code (ORC) 3724-03 Open Burning and Dumping, OAC 3745-27-05 Authorized,
Limited, and Prohibited Solid Waste Disposal Methods, and OAC 7345-54-13 general Waste
Analysis are applicable to off-site disposal. Any fuel blending of hazardous waste conducted on-
site in order to meet  operational and material handling parameters for off-site treatment facilities
will need to meet the substantive requirements for tanks set forth in 40 CFR Part 264 Subpart J.
These regulations deal primarily with the design of the tank and require that any tank in which
hazardous waste is placed must have sufficient structural integrity and corrosion protection such

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that it will not rupture, collapse, or leak.  If the material in the tank contains free liquid by the
paint filter test, SW-846 Method 9095, the requirements under the state equivalent of §264.193
for secondary containment and leak detection systems and the requirements for ignitable wastes
under §264.198 will also apply.
                                                              i
Off-site disposal for excavated soils which do not pass the TCLP will also require compliance
with the CERCLA Off-site Rule, 40 CFR 300.440, rules for Transporters of Hazardous Waste,
40 CFR Part 263, and the Land Disposal Restrictions of 40 CFR Part 268.  Waste which contains
CERCLA hazardous substances or pollutants or contaminants must be managed in a U.S. EPA
approved facility. If this waste is disposed of outside the United States, the rules pertaining to
Export of Hazardous Waste, 40 CFR Part 262 Subpart E, will apply rather than the Land
Disposal Restrictions.

Primary Balancing Criteria

3.     Long-term Effectiveness and Permanence

Both options meet the requirements of Long-term Effectiveness and Permanence.  Hot spot
excavation will quickly reduce the PAHg contamination to achieve the alternative 97 ppm PAHC
cleanup standard that would minimize risk to public health and the environment over the long-
term.  For in-situ bioremediation, even though it may be difficult, over the long-term and given
enough time it may be possible to achieve either the original .97 ppm PAHC or the alternative 97
ppm PAHC cleanup standards.  Ecological studies of the wetland restoration over time would
ensure that the habitat continues to pose no ecological threat.

4.     Reduction of Toxicitv. Mobility or Volume Through Treatment

In-situ bioremediation fully meets the criterion for reduction of Toxiciry, Mobility or Volume
Through Treatment.  Hot spot excavation and wetland development partially meets the criterion.
Off-site disposal of excavated soils would not reduce toxicity, mobility, or volume through
treatment. However, wetland development could potentially reduce low levels of contamination
left after excavation  by natural filtering processes occurring within the wetland.

5.     Short-term Effectiveness

In-situ bioremediation is partially effective in the short-term, while hot spot excavation is an
effective short term solution. Both require excavation and impacts to public health and the
environment are not anticipated due to the nature of PAHC compounds which do not volatize into
the air easily. In-situ bioremediation is considered less  effective in the short-term because it will
take a number of years to clean Lagoons 1-4 to either the original .97 ppm PAHC or the
alternative 97 ppm PAHC clean-up standards. Excavation and off-site disposal is effective in the
short term because it removes the contaminated soils immediately.

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6.     Implementabilitv

Hot spot excavation and wetland development fully meets the criterion for Implementability.
Excavation is known, easily applied engineering, while wetland development will require no
specific technology. However, in-situ bioremediation would be more difficult to implement due
to difficulty in distributing oxygen and nutrients through a series of trenches to the
microorganisms in the soils. The in-situ bioremediation pilot tests conducted at the site
identified this implementation problem. Results of the pilot tests indicate that in-situ
bioremediation may not actually be able to achieve the original .97 ppm PAHC or the 97 ppm
PAHC alternative cleanup standard in a timely manner.

7.     Cost

The cost of the in-situ bioremediation is $30 million. The cost of excavation and wetland
development is $1.2 million. The cost saving for changing the remedy from in-situ
bioremediation to hot spot excavation and wetland development in Lagoons 1-4 is approximately
$29 million.

Modifying Criteria

8.     State Acceptance

The Ohio Environmental Protection Agency (Ohio EPA) supports the hot spot excavation and
subsequent wetland development in Lagoons 1-4.

9.     Community Acceptance

Only public comments in support of the proposed plan were received during the public comment
period.
EVALUATION FOR LAGOON 5 REMEDY

The four options considered for remediation of Lagoon 5 included:

1.     On-site incineration of Lagoon 5 and the tarry soils;

2.     Construction of a RCRA Subtitle C containment cell in Lagoon 2 for the 122,000 cubic
       yards of material in Lagoon 5 and the tarry soils;

3.     Recycle back to coke plants the soft tar, which is classified as KO87 with the remaining
       coal/coke fines and hard tar in Lagoon 5 being used as an alternative fuel. If it appears
       that the capacity is not available at coke plants to recycle the K.O87, treatment and/or

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       disposal of the material off-site in an approved hazardous waste facility might be
       necessary. The 8,800 cubic yards of tarry soils on top of Lagoon 5 will be separated by
       screening into three types of material (tar, debris, and product for use in cement kilns).
       The tar will be used as an alternative fuel. The debris, which consists of clean brick and
       concrete, will be placed back on-site into the excavated Lagoon 5. Additional product
       from the tarry soils will be sent to cement kilns for use in their processes.; and

4.     Recycle back to coke plants the soft tar (KO87) and cap the remaining material in Lagoon
       5.
Threshold Criteria                                       '

1.     Overall Protection of Human Health and the Environment

All four options are protective of human health and the environment.  By utilizing containment
or excavation and treatment all four options will provide protection from contamination in
Lagoon 5, containment by preventing exposure to the contaminants and excavation by removing
the contaminants.

2.     Compliance with Applicable or Relevant and Appropriate Requirements (ARARs)

Compliance with applicable or relevant and appropriate requirements (ARARs) must be met for
all four options. Option 1 and 3 comply with all ARARs. Option 2 does not comply with OAC
3745-54-18, Location for Hazardous Waste Facilities.  Option 4 does not comply with OAC
3745-27-07, Other Criteria  for Solid Waste Disposal Facilities. Both options involve siting a
containment unit in a floodplain. Because Options 2 and 4 do not comply with ARARs they will
not be carried forward through the analysis.

For Options 1 and 3  off-site disposal in a landfill would require compliance with the State's
regulatory equivalent of RCRA 40 CFR Part 261, Toxicity Characteristics.  Toxicity
characteristic  leaching potential (TCLP) testing and analysis will help determine the off-site
disposal destination  of the excavated soils.  Ohio Revised Code (ORC) 3724-03 Open Burning
and Dumping, OAC 3745-27-05 Authorized, Limited, and Prohibited Solid Waste Disposal
Methods, and OAC 7345-54-13 General Waste Analysis are applicable to off-site disposal.  Any
fuel blending  of hazardous  waste conducted on-site in order to meet operational and material
handling parameters for off-site treatment facilities will need to meet the substantive
requirements  for tanks set forth in the state equivalent of 40 CFR Part 264 Subpart J. These
regulations deal primarily with the design of the tank and require that any tank in which
hazardous waste is placed must have sufficient structural integrity and corrosion protection such
that it will not rupture, collapse, or leak.  If the material in the tank contains free liquid by the
paint filter test, SW-846 Method 9095, the requirements under the state equivalent of §264.193
for secondary containment  and leak detection systems and the requirements for ignitable wastes

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                                          10

under the state equivalent of §264.198 will apply.
Off-site disposal for excavated soils which do not pass the TCLP will also require compliance
with the CERCLA Off-site Rule, 40 CFR 300.440, rules for Transporters of Hazardous Waste,
40 CFR Part 263, and the Land Disposal Restrictions of 40 CFR Part 268.  Waste which contains
CERCLA hazardous substances or pollutants or contaminants must be managed in an U.S. EPA
approved facility. If this waste is disposed of outside the United States, the rules pertaining to
Export of Hazardous Waste, 40 CFR Part 262 Subpart E, will apply rather than the Land
Disposal Restrictions.

Primary Balancing Criteria                             '

3.     Long-term Effectiveness and Permanence

Options 1 and 3 meet the requirements of Long-term Effectiveness and Permanence. Both
require excavation which will eliminate  the contamination from Lagoon 5.

4.     Reduction of Toxicity. Mobility or Volume Through Treatment

Option 1 would reduce toxicity, mobility, or volume through incineration of the materials in
Lagoon 5. Option 3 would reduce toxicity, mobility, or volume through any recycling of KO87
materials and the use of the other materials as an alternative fuel.

5.     Short-term Effectiveness

Options 1 and 3 are effective in the short-term. Engineering controls exist to control impacts to
public health and the environment due to volatization of any wastes during excavation in Options
1 and 3. Off-site recycling in Options 3  is effective in the short term because it removes the
contaminated soils immediately.

6.     Implementabilitv

Options 1 and 3 are fully implementable. Excavation is known, easily applied engineering.
Incineration is a proven technology at many sites. Recycling or off-site treatment and/or
disposal facilities that can accept the materials from Lagoon 5 and currently have the capacity to
handle the volume of material anticipated from Lagoon 5 exist.

7.     Cost

Present worth costs for Option 1  are $30.7 million. Option 3 present worth costs are $ 9 million.
The cost savings in changing the remedy for Lagoon 5 from Option 1  incineration to Option 3
recycling/alternative fuels is approximately $22 million.

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Modifying Criteria

8.     State Acceptance

The Ohio Environmental Protection Agency (Ohio EPA) supports Option 3 for remediation of
Lagoon 5.

9.     Community Acceptance

Only public comments in support of the proposed plan were received during the public comment
period.

IV.    DESCRIPTION OF THE SELECTED ALTERNATIVE

The selected revision for the 457,000 cubic yards of waste material in Lagoons 1-4 includes hot
spot excavation and wetland development. The hot spot excavation includes the use of an
alternative cleanup standard for carcinogenic PAIL, established in the 1990 ROD for the CPLA
operable unit. The 1990 ROD  provided an alternative cleanup standard of 97 ppm for PAH,, if
the chosen remedy of in-situ bioremediation could not achieve the original cleanup standard of
0.97 ppm in a timely manner. The selected change would achieve the 97 ppm alternative
cleanup standard with hot spot excavation of approximately 6,800 cubic yards of material.
Coal/coke fines and hard tar discovered during the excavation of Lagoons 1-4 will be used as an
alternative fuel. Soil  from the excavation will be disposed of off-site in a solid waste landfill if
the material is non-hazardous. If coal/coke fines, hard tar, or soils are determined to be
hazardous they will be treated and/or disposed of appropriately.

After excavation, a wetland ecology will be developed in the Lagoon area. To ensure that the
material remaining after the excavation is protective of ecological receptors, a wetland
development workplan and yearly ecological reconnaissance will be required.

The selected revision of the incineration of material from Lagoon 5 includes recycling of soft tar
back to coke plants, incineration of hard tar, off-site disposal of hard tar and debris commingled
with soft tar at an approved hazardous waste landfill, and the use of the remaining coal/coke fines
as an alternative fuel. Lagoon 5 contains soft tar and hard tar along with coal/coke fines and
debris. The soft tar, which is a tar decanter sludge from the coke plants, is KO87 listed waste.
Pursuant to RCRA regulations, KO87 listed waste may be recycled back to coke plants.  If it
appears that capacity is not available at coke plants to recycle the KO87, and the soft tar cannot
be recycled, it will be treated and/or disposed off-site in an approved hazardous waste facility.
Hard tar will be sent to an electric utility incinerator. Prior to shipment, testing must demonstrate
that the hard tar is non-hazardous through the use of the Toxicity Characteristic Leaching
Potential (TCLP) test. Some hard tar may be blended on-site to meet operational and material

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                                           12

handling requirements of the incinerator facility.  Any fuel blending of hazardous waste
conducted on-site in order to meet operational and m-terial handling parameters for off-site
treatment facilities will need to meet the substantive requirements for tanks set forth in the state
equivalent of 40 CFR Part 264 Subpart J. These regulations deal primarily with the design of the
tank and require that any tank in which hazardous waste is placed must have sufficient structural
integrity and corrosion protection such that it will not rupture, collapse, or leak. If the material in
the tank contains free liquid by the paint filter test, SW-846 Method 9095, the requirements
under the state equivalent of §264.193 for secondary containment and leak detection systems and
the requirements for ignitable wastes under the state equivalent of §264.198 will also apply.
Large debris and hard tar commingled with soft tar that does not meet the acceptance criteria of
the recycling facility will be disposed off-site at an approved hazardous waste landfill. The
coal/coke fines present in Lagoon 5 will be used  as an alternative fuel for boilers.  Prior to its
use as an alternative fuel, testing must demonstrate that  the fines are non-hazardous through the
use of the Toxicity Characteristic Leaching Potential (TCLP) test. If the alternative fuel is
hazardous, it will be treated and/or disposed in an approved hazardous waste facility.
Uncontaminated brick and concrete uncovered during the excavation of Lagoon 5 will be used as
clean fill in Lagoon 5.  Other types of debris discovered during the excavation will be disposed
of off-site in an approved landfill.

The 8,800 cubic yards of tarry soils on top of Lagoon 5 will be separated by screening into three
types of material (tar, debris, and product for use in cement kilns). The tar will be used as an
alternative fuel. The debris, which consists of clean brick and concrete, will be placed back on-
site into the excavated Lagoon 5. Additional product from the tarry soils will be sent to cement
kilns for use in their processes. Other types of debris excavated from Lagoon 5 will require
disposal off-site in a landfill. The 30,000 cubic yards of site soils which was excavated near the
former coke plant will also be placed in the Lagoon 5 excavation to achieve grade for the wetland
development.

V.     STATUTORY DETERMINATIONS

The off-site transport and disposal of waste containing hazardous materials without treatment is
the least favored alternative remedial action where practicable treatment technologies are
available. Based upon new information that the materials in Lagoons 1-4 are not as
contaminated as previously thought and that the bioremediation will not achieve clean-up in a
timely manner, changing the remedy for Lagoons 1-4 to hot spot excavation and wetland
development is justified. Hot spot excavation is readily implementable and will achieve the
alternate cleanup standard identified in the 1990 ROD for the CPLA operable unit in a
substantially shorter timeframe than bioremediation.

The remedial options for lagoons 1-4 are roughly equivalent in complying with the nine criteria,
with the selected option slightly preferable. Both are protective and comply with ARARs.
While the hot  spot excavation and wetland development only partially meets the criteria for
Reduction of Toxicity, Mobility, and Volume Through Treatment, the removal, off-site disposal,

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                                          13

and wetland development are effective technologies that are readily implementable as opposed to
in-situ bioremediation, which is difficult to implement and, based on pilot studies, questionably
effective.  In addition, cost savings associated with the change are substantial, with the hot spot
excavation and wetland development potentially more effective in reducing contamination at a
reduced cost.

For Lagoon 5 waste material, the incineration and recycling/alternative fuels options fully meet
all the criteria and are comparable; however, the recycling/alternative fuels option is easier to
implement, can be completed in a timeframe that is two years'shorter than incineration, and
result in a cost savings of over $20 million. The recycle option also treats and disposes of the
Lagoon 5 material off-site which is easier to implement than incineration on-site. Therefore,
modifying from the incineration option to the recycling/alternatives fuels option is justified.

Off-site disposal and treatment of soils from Lagoons 1-5 is protective of human health and the
environment since the soils will  be managed in appro /ed facilities. Remaining soils will meet
the PAHC alternative cleanup standard or be at a depth which will not affect human health or the
environment. The use of recycling, treatment and/or disposal of the Lagoon 5 materials does
satisfy the statutory preference for treatment as a principal element of the remedy and employs
permanent solutions and alternate treatment technologies to the maximum extent possible.

Compliance with ARARs, specifically the State equivalent of RCRA 40 CFR Part 260 to 271,
ORC 3734-03, OAC 3745-27-05, and OAC 3745-54-13 will be met with off-site disposal of the
Lagoon soils. Disposal of soils containing CERCLA hazardous substances must meet the
CERCLA Off-Site Disposal Rule, 40 CFR 300.440 and the Land Disposal Restrictions, 40 CFR
Part 268. If this waste is disposed of outside the United States, the rules pertaining to Export of
Hazardous Waste, 40 CFR Part 262 Subpart E, will apply rather than the Land Disposal
Restrictions. In addition, any fuel blending of hazardous waste conducted on-site in order to
meet operational and material handling parameters for off-site treatment facilities will need to
meet the substantive requirements for tanks set forth in the state equivalent of 40 CFR Part 264
Subpart J.  These regulations deal primarily with the design of the tank and require that any tank
in which hazardous waste is placed must have sufficient structural integrity and corrosion
protection such that it will not rupture, collapse, or leak. If the material in the tank contains free
liquid by the paint filter test, SW-846 Method 9095, the requirements under the state equivalent
of §264.193  for secondary containment and leak detection systems and the requirements for
ignitable wastes under the state equivalent of §264.198 will also apply. The two changes
outlined in ROD Amendment #3 could result in a total savings of approximately $50 million.

VI.    DOCUMENTATION OF SIGNIFICANT CHANGES

One of the provisions of the Proposed Plan for ROD Amendment #3 addressed the type of
treatment for the material from Lagoon 5.  Some of the material in Lagoon 5, specifically the soft
tar, K.O87, has been identified by the U.S. EPA as a principal threat, and the preference is for
treatment of these materials. The Proposed Plan recommended the recycling of soft tar back to

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                                            14

coke plants and the use of the remaining coal/coke fines and hard tar as alternative fuel. The
Proposed Plan also identified that, if the soft tar could not be recycled, due to capacity at coke
plants or other reasons, the soft tar would be treated and/or disposed off-site in an approved
hazardous waste facility.

During the development of ROD Amendment #3, the potentially responsible party pursued
contracting for the recycling option as well as incineration (offsite or onsite) of the KO87 soft tar
waste. The contracting activities determined that the capacity of the facilities which could accept
the soft tar was so limited that recycling could take from 4 to 6 extra years to complete and that
incinerating the soft tar could take from 2 to 2 V* extra years to complete. As a result, soft tar
would need to be stored on site for long periods, and the completion of the remedy would be
substantially delayed.  In addition, the potential high ash content of the soft tar due to its mixing
with other debris in the Lagoon 5 landfill, resulted  in many  of the off-site recycling and
commercial incinerator hazardous waste facilities being unable to accept the material because of
their quality specifications.  As a consequence, U.S. EPA estimates that a portion of the soft tar
cannot actually be recycled.

To examine recycling and treatment options further the responsible party excavated about 20 yd3
of tar material from Lagoon 5 to have it analyzed by the few recyclers and treatment facilities that
expressed interest in accepting the materials.  During the excavation it was discovered that
separating the soft and hard tar was more difficult than originally anticipated. However, the
responsible party was able to separate a variety of relatively unique waste streams and examined
treatment and disposal options for each. The waste streams included: "clean" soft tar, which is
primarily KO87 hazardous waste; non-commingled hard tar; large debris commingled with
KO87; "dirty" soft tar, which is KO87 waste mixed with hard tar, coal/coke fines, and ash; and
coal/coke fines. Treatment and disposal options included: the Acme Recycling Center, a coke
oven in Chicago, Illinois; a commercial cement kiln incinerator called Giant Resource Recovery
Co.; a non-hazardous electric utility incinerator called Baldwin Thermal Treatment in Baldwin,
Illinois;  Safety Kleen (Laidlaw) landfill in Corunna, Canada; and alternative fuel sources for the
coal/coke fines. Representatives from these facilities visited the Ironton site to perform on-site
inspections and collect waste profiles. After visiting the site, Giant Resource Recovery was
eliminated as an option because their acceptance criteria and quality requirements could not be
met by the materials present in Lagoon 5.

After receiving feedback from each of the potential disposers, a receptor for each waste stream
was identified.  "Clean" soft tar, which is KO87 waste that  meets the, acceptance criteria and
quality requirements to be recycled for use in coke ovens, will be shipped to Acme.  The only
limiting factor is the capacity of the recycler to accept the waste. If the recycler's capacity is
delaying the excavation, "clean" soft tar will  be disposed at Laidlaw in Canada until the issues
are resolved.  Non-commingled hard tar will be sent to Baldwin.  Prior to shipment, testing
must demonstrate that the hard tar is non-hazardous through the use of the Toxicity
Characteristic Leaching Potential (TCLP) test.  Some hard  tar may be  blended on-site to meet
operational and material handling requirements of the incinerator facility. Large debris

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                                           15

commingled with KO87 will be sent to Laidlaw. "Dirty" soft tar will be sent to Acme unless it
does not meet their acceptance criteria and quality requirements, i.e. fine contents and debris size,
in which case it will disposed off-site at Laidlaw.  Coal/coke fines, which is the bulk of material
in Lagoon 5, as mentioned previously, will be used as an alternative fuel. Presently, there are a
number of facilities interested in and have the capacity to handle the coal/coke fines.

The ARARS for this modification of ROD Amendment #3 remain those described in the
discussion of ARARS for that ROD Amendment.

Therefore, U.S. EPA is clarifying the remedy selected in ROD Amendment #3 to off-site
recycling of the "clean" soft tar at the Acme facility. Hard tar will be treated off-site at the
Baldwin facility.  Coal/coke fines will be used as an alternative fuel. The remaining material
including  large debris commingled with KO87 waste and "dirty" soft tar which fails to meet the
specifications for recycling will be disposed off-site in compliance with State and Federal
hazardous waste regulations. It is currently anticipated that this last category of material would
be sent to a facility operated by Laidlaw Corporation in Corunna, Canada.  As part of the off-site
disposal at the Canadian facility, following stockpiling of the material, samples will be collected
for analytical testing for parameters required by the disposal facility. These tests will be
performed to determine a 15 psi penetration. This is a compressibility standard established by
the facility to aid in material placement options. It may become necessary to stabilize the
material to meet the compressibility standard and because at different times during the removal
of the soft tar handling the material may be difficult due to warm weather and fluidity of the tar.
Cement or fly ash will be added as a stabilizing agent.  The stabilization will generally be
performed in the lagoon area; however, it may become necessary to perform the mixing process
in vessels near where the soft tar material will be stockpiled for shipment.

This modification in the selected remedy will not fundamentally alter the selected remedy with
respect to scope, performance or cost.  The same amount of soft tar, hard tar, and coal/coke fines
will be removed from Lagoon 5 and managed off-site.  Lagoon 5 will still be excavated, some
soft tar will be recycled,  the hard tar will still be treated, coal/coke fines will still be used as an
alternative fuel, and uncontaminated debris will still be used either in cement kilns or placed
back on-site into the excavated Lagoon 5, as approved in ROD Amendment #3.

Although the off-site disposal of some of the soft tar only partially meets the criteria for
reduction of toxicity or volume through treatment, it does provide greater short term
effectiveness and  is more implementable than recycling and incineration. The requirements for
off-site disposal can be easily met, eliminating concerns with the "quality" of the soft tar and its
acceptability at a recycling facility. In addition, the schedule for completion of the selected
remedial action will be maintained. The modification to off-site disposal is in compliance with
ARARs and the State of Ohio has been informed of the modification and concurs.  On-site
blending of hard tar to meet operation and material handling requirements of the off-site
incinerator will meet the substantive requirements of the state  equivalent of 40 CFR Part 264
Subpart J.  Overall cost and timeframes of the project are hard to estimate given the various

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                                           16

waste streams and treatment/disposal options. Some recent figures submitted by the PRP which
examined the costs of incineration, recycling, or off-site disposal of just the soft tar material
ranged from $5.9 million for the off-site disposal to $8.1 million for incineration. Costs are
expected to fall within this range. Timeframes were also examined and ranged from 13 months
to complete to 2 years for the incineration and over 5 years for the recycling option. Timeframes
are expected to  fall between 13 months and 2 years.

Information pertaining to this modification will become part of the administrative record file
located at Briggs Lawrence County Library, located in Ironton, Ohio.

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                                                      DRAWN I	CS
                                                                         LAGOON 3
                    COKE
                        AR
                                                                                             COKE  PLANT AND
                                                                                               LAGOON  AREAS
                                                                                                PREPARED FOR
                                                                                              ALLIEDSIGNAL INC.
                                                                                          MORRISTOWN. NEW JERSEY
                                                                                                   INTERNATIONAL
                                                                                                   TECHNOLOGY
                                                                                                   CORPORATION
© t984 IT CORTOR* T\0n
  LL COPYRIGHTS RESERVED
  •Do Mol Scd4 Dik OrairXg'

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                        0.S. ENVIRONMENTAL PROTECTION AGENCY
                                   REMEDIAL ACTION

                               ADMINISTRATIVE RECORD
                                         FOR
                     ALLIED CHBMICAL/IRONTON COKE SUPBRFUND  SITE
                           IRONTON, LAWRENCE COUNTY,  OHIO

                      OPERABLE UNIT #2: COKE PLANT/LAGOON AREA
                                     UPDATE #9

                                  DECEMBER 3,  1997
NO.   DATE

 1    00/00/00
AUTHOR

AlliedSignal,
Inc.
RECIPIENT

U.S. EPA
                                                                              PAGES
      00/00/(J£    AlliedSignal,      U.S.  EPA
 3    00/00/00
 4    00/00/00
 5    00/00/00
AlliedSignal,
Inc.
AlliedSignal,
Inc.
AlliedSignal,
Inc.
U.S. EPA
U.S. EPA
U.S. EPA
 6    00/00/00
 7    06/22/92
U.S. EPA
Federal
Register
File
 Public
Drawing:  Ironton Coke
Plant Lagoon No.  5
Field Characterization:
Visual Analysis  of
Tar Materials

.Dcauing:  Ironton Coke
Plant LagJon No.  5
Field Characterization:
Boring Locations

Drawing:  Ironton Coke
Plant Lagoon No .  5
Field Characterization:.
Benzene Analysis of
Materials

Drawing:  Ironton Coke
Plant Lagoon No.  5
Field Characterization:
Proposed  Boring
Locations

Drawings :  Ironton Coke
Plant Lagoon No.  5
Boring Locations,-
Visual Analysis  of Tar
Materials;  HNU Analysis
Of Materials;  Benzene
Analysis  of Materials

Outline  re: Removal
Options  and Criteria
at  the Allied Chemical/
Ironton  Coke  Site

40  CFR  Parts  261, 266,
and 271:  Hazardous Waste
Management System;
 Identification and
 Listing of Hazardous
 Waste;  Exclusions; Final
 Rule (FR: Vol.  57, No.
 120;  pp. 27880-27888)
10

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                                                    Allied Chemical/Ironton  Coke  AR
                                                                   Operable  Unit  *2
                                                                           Update  #9
                                                                              Page 2
      DAIB
            AUTHOR
                              RECIPIENT
                                    TITLE/DESCRIPTION
                                                                        PAGES
 8     08/18/92    Federal
                              Public
      08/09/96
10
08/23/96
            Lewis, M.,
            AlliedSignal,
            Inc.
Ford, R.,
AlliedSignal,
Inc.
11
12
09/30/96
11/11/96
Ohio EPA
Lewis, M.,
AlliedSignal,
Inc.
13
11/13/96
14
11/21/96
Lewis, M.,
AlliedSignal,.
Inc.
Ford, R.,
AlliedSignal,
Inc.
                  Alcamo, T.,
                  U.S. EPA and
                  K. Gilmer,
                  Ohio EPA
Alcamo, T.,
U.S. EPA and
K. Gilmer,
Ohio EPA
                                    U.S. EPA
Alcamo, T.,
U.S. EPA and
K. Gilmer,
Ohio EPA
Alcamo, T.,
U.S. EPA and
K. Gilmer,
Ohio EPA
                                    Alcamo, T.,
                                    U.S.EPA and
                                    K. Gilmer,
                                    Ohio  E-PA
 40 CFR Parts 261 et al:     24
 Identification and
 Listing of Hazardous
 Waste; CERCLA Hazardous
 Designation; Reportable
 Quality Adjustment;
 Coke By-Products Waste
 (FR:  Vol.57,  No.  160;
 pp.  37284-37306)

 Letter:  K087 Remediation    4
 Alternative Costs for
 the  Coke Plant/Lagoon
     _ Operable Unit at
   e AllieH" Chemical/
 Ironton  Coke Site

 Letter re:  Allied's        20
 Request  for U.S.  EPA/
 OEPA's Review of
 Attached Peti tion .to
 Amend the Record of
 Decision for the
 Ironton  Coke Plant
 CP/LA Operable Unit

 Construction and           108
 Demolition Debris Rules
 (Chapters 3745-37 and   -
 3745-400 of the Ohio
 Administrative Code)

 Letter Forwarding           2
 Attached Drawing  re:
 Conceptual Design of
 a  Hazardous Waste Cell
 in Lagoon 4 at the
 Allied Chemical/Ironton
 Coke Site

 Letter re: Access Road      2
 Between  the Cell and
 Floodwall Berm at the
 Allied Chemical/Ironton
 Coke Site w/Attached
• Drawing

 Letter Forwarding            2
 Attached Table re:
 Cost Estimates for
 Lagoon  5 Options  at the
 Allied Chemical/Ironton
 Coke Site

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                                                    Allied Chemical/Ironton Coke AR
                                                                   Operable Unit #2
                                                                          Update #9
                                                                             Page 3
HO.

15    11/21/96
16
      12/13/96
17
                  AUTHOR

                  Ford,  R.,
                  AlliedSignal,
                  Inc.
Ford, R.,
AlliedSignal,
Inc.
                 •Bewis,"M.,
                  AlliedSignal,
                  Inc.
18
      01/17/97
19
      02/20/97
Arbesman, P.,
AlliedSignal,
Inc.
AlliedSignal,
Inc.
20
      03/13/97
U.S. EPA
21
      03/14/97
 Internat ional
 Technology
 Corporation
                  RECIPIENT

                  A]cano,  T.,
                  U.S. EPA and
                  K. Gilmer,
                  Ohio EPA
Alcamo, T.,
U.S. EPA and
K. Gilmer,
Ohio EPA
                  Alcamo, T.,
                  U.S. EPA
                                                      TITLB/DB9CRIPTION       PAGES
Muno, W.,
U.S. EPA
                                    U.S.  EPA
                                    File
                                    U.S. EPA
 Letter Forwarding
 Attached Table re:
 Carcinogenic PAH Levels
 within Lagoons 1-4 at
 the Allied Chemical/
 Ironton Coke Site

 Letter Forwarding
 Attached Drawing re:
 Proposed Lagoon 5 Area
 Cell at the Allied
 Chemical/Ironton Coke
 Site

'COVer Letter Forwarding
 Boring Logs,  Trench Logs,
 Boring and Trench
 Location Drawing and
 Photographs from the
 August 1993 WFR Predesign
 Investigation at the
 Allied Chemical/Ironton
 Coke Site

 Letter re: Allied's
 Petition to Amend the
 Record of Decision for
 the Allied Chemical/
 Ironton Coke Site

 Drawing: Proposed
 Sampling Locations for
 the Lagoon Materials
 Delineation Program at
 the Allied Chemical/
 Ironton Coke Site

 Outline of Proposed
 Lagoon 5  Field Charac-
 terization at the
 Allied Chemical/Ironton
 Coke Site  (DRAFT)

 Letter Forwarding
 Attached  Draft  Lagoon
 Materials Delineation
 Workplan  for  the Coke
 Plant/Lagoon  Area at
 the Allied Chemical/
 Ironton  Coke  Site
                                              16

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                                                    Allied Chemical/Ironton Coke AR
                                                                   Operable Unit #2
                                                                          Update #9
                                                                             Page 4
22
PATH

03/31/97
AOTHOR

Shott, D.,
International
Technology
Corporation
23    06/23/97
            Ford, R.,
            AlliedSignal,
            Inc.
24
07/15/97
                  Alcamo,  T.,
                  U.S. EPA
25
08/13/97
26
08/28/97
27
10/03/97
Shott,  D.,
International
Technology
Corporation
Shott, D.,
International
Technology
Corporation
Alcamo, T.,
U.S. EPA
28
10/14/97
Lewis, M.,
AlliedSignal,
Inc.
RBCIPTJHMT

Alcamo,  T.,
U.S. ^PA and
K. Gilmer,
Ohio EPA
                  Alcamo, T.,
                  U.S. EPA and
                  K. Gilmer,
                  Ohio EPA
                  Ford,  R.,
                  AlliedSignal,
                  Inc.
                                    Alcamo,  T.,
                                    U.S.  EPA and
                                    K.  Gilmer,
                                    Ohio EPA '
                                    U.S. EPA
Gilmer, K.,
Ohio EPA
                                    Alcamo, T.,
                                    U.S. EPA and
                                    K. Gilmer,
                                    Ohio EPA
 TITLK/D83CRIPTION       PAGES

 Letter Forwarding           3
 Attached (1)  Revised
 Page  1 and (2)  Revised
 Figure 1:  Proposed
 Sampling Locations for
 the Draft  Lagoon
 Materials  Delineation
 Workplan for  the Allied
 Chemical/Ironton Coke
 Site

 Letter Forwarding           8
 Attached (1)  Revised
 Table  3: Lagoon 1-4
.SxM^jle Points and (2)
 Sample Location Map
 for the AlliedSignal
 Coke Plant/Lagoon Area
 Site

 Letter re:  the  Lagoon       2
 Area Carcinogenic Poly-
 Nuclear Aromatic Hydro-
 Carbons (PAH) Data Table
 for Lagoons 1-4 at the
 Allied Chemical/Ironton
 Coke Site

 Letter Forwarding           7
 Attached Revised PAH
 Data Table and  Sample
 Location Map  for the
 Allied Signal Coke
 Plant/Lagoon  Area Site

 Letter Forwarding         23
 Attached Summary of
 Data  from the May-June
 1997  Lagoon No   5 Field
 Characterization Program
 at the Allied Chemical/
 Ironton Coke  Site

 Letter re: Tar  Decanter    3
 Sludge  (K087) within
 Lagoon 5 and Different-
 iating Between  Hard Tar
 and  Soft Tar at  the
 Allied Chemical/Ironton
 Coke Site

 FAX  Transmission         4
 Forwarding Attached
 October 7, 1997  Draft
 Meeting Notes  re:
 AlliedSignal/Ironton
 Coke Site

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                                                    Allied  Chemlcal/Ironton Coke XR
                                                                   Operable Unit ft 2
                                                                          Update #9
                                                                             Page 5
NO.   PATH

29    10/27/97




30    10/28/97




31    10/29/9.7
            MOTOR.'

            Lewis, M.,
            AlliedSignal,
            Inc.
            Ford,  R.,
            AlliedSignal,
            Inc.
            Lewis, M.,
            AlliedSignal,
            Inc.
32    11/04/97    Moschell,  M.,
                  Ohio EPA
33
11/05/97
34
11/10/97
Shott,  D.,
International
Technology
Corporation
Muno, w.,
U.S. EPA
 35     12/01/97    Lewis. M.,
                  AlliedSignal,
                  Inc.
                  RKCIPTBNT

                  Alcamo,  T.,
                  U.S.  EPA and
                  K.  Gilmer,
                  Ohio  EPA

                  Alcamo,  T.,
                  U.S.  EPA
                  Alcamo,  T.,
                  U.S.  EPA and
                  K.  Gilmer,
                  Ohio  EPA
                             Gilmer, K.,
                             Ohio EPA
Alcamo,  T.,
U.S. EPA and
K. Gilmer,
Ohio EPA
Arbesman, P.,
AlliedSignal,
Inc.
                              Alcamo,  T.,
                              U.S. EPA and
                              K. Gilmer,
                              Ohio EPA
                  TITIiH/DBSCmPTION

                  Letter re: Tarry Soils
                  Pile at Lagoon 5 at the
                  Allied Chemical /Ironton
                  Coke Site

                  Letter re: Origin of
                  Waste Tar in Lagoon 5
                  at the Allied Chemical/
                  Ironton Coke Site
                                                                              PAijBS
.
Forwarding"" Attached
Table re : Summary  of
Hazardous Characteristic
Testing for Tarry  Soils
at the Allied  Chemical/
Ironton Coke Site

Memorandum re:  Allied's  '
Hazardous Waste Determin-
ation for Hard Tar at
the Allied Chemical/
Ironton Coke Site

Letter re : Summary of
the May 27 - June  12,
1997 Lagoon No. 5  Field
Characterization Program
at the Allied  Chemical/
Ironton  Coke Site

Letter  re: U.S. EPA's
Review  of  Allied's
August  23,  1996 Petition
to Amend the  December
 1990  Record of Decision
 for  the Coke  Plant/
 Lagoon Area at the
Allied Chemical /Ironton
 Coke Site
 \
 Letter re: Estimated
 Costs for the  Allied
 Chemical /Ironton  Coke
 Site w/Attached Lagoon
 No.  5 Proposed Final
 Grading Plan  Drawing

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                        U.S. ENVIRONMENTAL PROTECTION AGENCY

                               ADMINISTRATIVE RECORD
                                         FOR
                          ALLIED CHEMICAL/IRONTON COKE  SITE
                                  OPERABLE UNIT #2
                           IRONTON, LAWRENCE COUNTY, OHIO

                                     UPDATE #10
                                 SEPTEMBER 29, 1998
NO.   DATE

 1    12/00/97





 2    07/21/98





 3    09/16/98
 4    00/00/00
AUTHOR

U.S.. EPA
Hunt, M. ,
AlliedSignal,
Inc.
Hunt,  M.,
AlliedSignal,
Inc.
U.S. EPA
RECIPIENT

Public
Mankowski, M.,
U.S. EPA
Mankowski,  M.,
U.S. EFA
Public
T, ITT.H /OBSCRIPTIQN       PAGES

Fact Sheet: Proposed        12
ROD Amendment  #3 for
the Allied Chemical/
Ironton Coke Site

Letter re: Lagoon 2/5       21
Remediation at the Allied
Signal/Ironton Coke Site
w/ Attachments

Letter re: Lagoon 2/5       90
Remediation (Tar Excava-
tion/Disposal) at the
AlliedSignal/Ironton
Coke Site w/ Appendices
I-XI)

Record of Decision Amend-
ment for Operable Unit
#2 at the Allied Chemical/
Ironton Coke Site
(PENDING)

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