ORP/EERF 73-3 PORTABLE ANNEALER FOR THERMOLUMINESCENT DOSIMETERS U.S ENVIRONMENTAL PROTECTION AGENCY Office o* Radiation Programs ------- OFFICE OF RADIATION PROGRAMS EASTERN ENVIRONMENTAL RADIATION FACILITY TECHNICAL REPORTS Technical reports of the Eastern Environmental Radiation Facility are available from the National Technical Information Service, Springfield, Virginia 22151, when a PB number is indicated after the title. Microfiche copies are $0.95; prices for paper copies are indicated after the PB number. Bulk order prices are available from NTIS. The PB number should be cited when ordering. Title Radiological Survey of Major California Nuclear Ports (April 1967) (PB 178 728 $6.00) BRH/SERHL 70-1 RO/EERL 71-1 EERL 71-2 ORP/EERF 73-1 ORP/EERF 73-2 ORP/EERF 73-3 Radiological Survey of Hampton Roads, Virginia (January 1968) (AD 683 208 $6.00) Laboratory Examination of a Ruptured 50-mg Radium Source (May 1970) (PB 191 810 $3.00) Development of Ion Exchange Processes for the Removal of Radionuclides from Milk (January 1971) (PB 198 052 $0.50) Investigation of Tritiated Luminous Compounds (June 1971) Suitability of Glass-Encapsulated Thermoluminescent Dosimeters for Environ- mental Radiation Surveillance (June 1973) Construction and Operation of an Ion Exchange Cartridge for Monitoring Radio- nuclides in the Environment (June 1973) Portable Annealer for Thermoluminescent Dosimeters (June 1973) ------- ORP/EERF 73-3 PORTABLE ANNEALER FOR THERMOLUMINESCENT DOSIMETERS S. T. Windham H. L. Kelley T. K. Plant Eastern Environmental Radiation Facility P. 0. Box 61 Montgomery, Alabama 36101 Author's present addresses: 1. Eastern Environmental Radiation Facility 2. Eastern Environmental Radiation Facility 3. University of Illinois June 1973 \ ENVIRONMENTAL PROTECTION AGENCY Office of Radiation Programs Waterside Mall East 401 M Street, S.W. Washington, D.C. 20460 ------- The mention of commercial products, their source, or their use in connection with material reported herein is not to be construed as either an actual or implied endorse- ment of such products by the U. S. Environmental Protection Agency. 11 ------- FOREWORD The Eastern Environmental Radiation Facility participates in the identification of solutions to problem areas as defined by the Office of Radiation Programs. The-Facility provides laboratory capability for evaluation and assess- ment of radiation sources through environmental studies and surveillance and analysis. The EERF provides technical assistance to the State and local health departments in their radiological health programs and provides special laboratory support for EPA Regional Offices and other federal government agencies as requested. Charles R. Porter Acting Director Eastern Environmental Radiation Facility 111 ------- CONTENTS Page Foreword ii List of Figures iv Introduction 1 General Description 1 Circuit Description , 2 Performance Characteristics 2 Parts List 5 Summary 6 ------- FIGURES Page 1. Portable TLD Annealer 3 2. Schematic of Portable TLD Annealer 4 VI ------- PORTABLE ANNEALER FOR THERMOLUMINESCENT DOSIMETERS ORP/EERF-73-3 S. T. Windham, H. L. Kelley, T. K. Plant INTRODUCTION The requirement for low-level environmental radiological monitoring has led to the development and widespread use of thermoluminescent dosimeters (TLD's) for this purpose. TLD's offer a sensitive and accurate means for integrating exposures over extended periods of time, and are especially well suited for determining environmental radiation levels in the vicinity of nuclear facilities. The EERF, as well as several other organizations, has used the EG&G TL-15 TLD for environmental radiological monitoring. The TL-15 is "read out" by applying a current to the heating element within the dosimeter and measuring the light output from the CaF2:Mn chips. For the magnitude of exposure normally found in environmental monitoring for exposure periods of one month and in general for exposures below 200 mR, the "read out" process is adequate to anneal or dedose the dosimeter and permit reuse with no further annealing. Immediately prior to placing dosimeters in the field for a monitoring period, it is necessary to anneal dosimeters if they have been shipped and possibly exposed, or if some time has elapsed since they were last annealed. To avoid unnecessary shipment of the reader or an annealing oven into the field for this purpose, a small, portable annealer was designed and built by the Electronics Instrumentation Section at the Eastern Environmental Radiation Facility. This report describes the design and operation of the annealer. GENERAL DESCRIPTION In function the annealer performs similar to the heating circuit of the EG&G TL-3 reader, but without the photomultiplier tube and associated recording and control circuitry. The TL-3 reader uses a heating time of 13 seconds and a current of 6.5 amperes to "read out" the TL-15 dosimeter. Likewise, the annealer delivers a regulated current through the heating element of the TLD for a selected length of time. The heating time is adjustable from 0-30 seconds and the current is adjustable from 3-7.5 ------- amperes. A meter is used to aid in adjusting the current to the desired value. With the current and time easily adjustable, it is possible to use the instrument to anneal vacuum tube dosimeters of other manufacturers simply by changing the socket in which the dosimeter is inserted for annealing. A principal consideration in the design of the annealer was to produce a small, portable instrument. The final design, as seen in figure 1, will easily fit into an attache case with room remaining for dosimeters and other accessories. CIRCUIT DESCRIPTION The annealer consists of a timer and a current regulated power supply (figure 2). The timer is not necessary to the operation of the circuit, but aids in obtaining consistent annealing results. The operation of the current regulator is quite simple. A phase control circuit consisting of R3, GI, the diac, and the triac delivers power to the primary winding of T]_, a 110 VAC transformer with a 6.3 volt, 10 ampere secondary. RS and GI have been chosen such that the triac is conducting during most of the cycle. When the anneal circuit is first energized, essentially full voltage (6.3 VAC) is produced on the secondary. Unlimited, this surge would burn out the TLD being annealed, but the drop across Ry illuminates lamp 13. The normally high resistance of photocell R4 is quickly lowered which reduces the average conduction time of the triac. This reduces the current through the secondary of TI, but maintains a constant value depending on the setting of Rg. This constant current value is independent of the resistance of the TLD heating element due to the negative feedback action obtaine with the module containing 13 and R4. RS is a thermal resistor which acts to decrease the initial surge of current and thereby damps excessive meter movement. PERFORMANCE CHARACTERISTICS The manufacturer of the TL-15 dosimeter recommends a heating current of 6.5 amperes which was used through- out the performance tests of the annealer. To determine the minimum time required to dedose a dosimeter using the annealer, a group of dosimeters was exposed to 11.1 mR, ------- 0 3456 Front panel of annealer Inside view Figure 1. Portable TLD Annealer ------- 115V 60 Hz A.C. 0-10AA.C. P, Figure 2. Schematics of Portable TLD Annealer. ------- PARTS LIST Cx - .05 yF I, , I2 - neon indicator lamps F - 1 amp slo-blow fuse I3r £4 ~ Clairex CLM 3006A Photo Mod Sj_ - SPST Power-On Switch S2 - SPST Momentary Contact T>L - 110 VAC Primary 6.3 volt 10 amp secondary GE ST2 - Diac trigger diode GE SC 40B - Triac Switch Rl' R2 ~ 48k ohm, 1/4 watt resistors RO - 68k ohm, 1/2 watt resistor Re - Glow-Bar Surge Arrester Rg - 250 ohm, 2 watt resistor R7 - 0.5 ohm, 100 watt resistor P - appropriate socket for TLD being used M-, - 0-10 ampere AC meter Timer - 0-30 second instant reset timer ------- heated in the annealer, and "read out" using the TL-3 reader. The minimum time required for complete annealing was found to be 15 seconds. This annealing technique 6.5 amperes for 15 seconds, was accepted as the routine procedure used with the TL-15 dosimeter. For dosimeters which have been exposed to greater than 50 mR, EG&G recommends an oven annealing procedure instead of depending on the reader to dedose the^dosimeters. To determine the effectiveness of the annealer in dedosing exposures greater than 50 mR, several groups of dosimeters were given known exposures, heated in the annealer, and "read out" to determine any residual exposure. The following data were obtained: Annealing Effectiveness 6.5 amperes 15 seconds Delivered Residual reading Percent exposure after annealing annealed 232 mR 0 mR 100% 400 mR 0.14 mR 99.97% 872 mR 0.24 mR 99.97% 1760 mR 0.40 mR 99.97% From this it is seen that for normal environmental levels, less than 200 mR, the annealer is totally effective in dedosing the dosimeters. For exposures greater than this negligible residual exposure remains after annealing. For most applications this small residual exposure will be insignificant. If total annealing is necessary at these higher levels, an oven annealing procedure may be used or, possibly, longer heating times. SUMMARY The annealer described has been in use for several months with good results and no malfunctions. Components used in construction of this compact annealer are readily available and construction requires no special skills or equipment. The cost of building the annealer, less than $75 including the optional timer, represents a significant savings compared to the repair cost and down time should damage to the TLD reader occur during shipment to monitoring sites. Use of the annealer makes unnecessary a number of these shipments. ------- The effectiveness of the annealer in dedosing the TL-15 dosimeter was demonstrated. For exposures less than 200 mR, annealing was 100%. Thus the annealer has proven to be most adequate for environmental measure- ment work. US. Government Printing Office: 1973 - 743 - 901/7768 Region No. 4 ------- |