PB86-173606
THE LUBBOCK LAND TREATMENT SYSTEM RESEARCH AND
DEMONSTRATION PROJECT:   VOLUME II.   PERCOLATE
INVESTIGATION IN THE ROOT ZONE
Texas Tech University
Lubbock, TX
Feb 86
                U.S. DEPARTMENT OF COMMERCE
             National Technical Information Service

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&EPA
           United States
           Environmental Protection
           Agency
           Robert S. Kerr Environmental
           Research Laboratory
           Ada OK 74820
EPA/600/2-86/027b
February 1986
           Research and Development
The Lubbock Land
Treatment System
Research and
Demonstration
Project:

Volume II.
Percolate
Investigation in the
Root Zone

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                                   TECHNICAL REPORT DATA
                            (Please read Instructions, on the reverse before completing)
 i. REPORT NO.
 EPA/600/2-86/027b
                              2.
                                      3. RECIPIENT'S ACCESSION-NO.
                                          PBS 6   17.3bOf,
4. TITLE AND SUBTITLE
  THE LUBBOCK LAND TREATMENT SYSTEM RESEARCH AND
  DEMONSTRATION  PROJECT:  Volume II. Percolate
  Investigation  in the  Root Zone
                                      5. REPORT DATE
                                       February  1986
                                      6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S)
 R.H.  Ramsey and R.M. Sweazy
                                                           8. PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AND ADDRESS
                                                           10. PROGRAM ELEMENT NO.
 Texas  Tech University
 Lubbock,  TX  79409
    In  cooperation with:  Lubbock  Christian College
      Institute of Water Research,  Lubbock, TX  79407
                                       CAZB1B
                                      11. CONTRACT/GRANT NO.
                                       CS-806204
 12. SPONSORING AGENCY NAME AND ADDRESS
  U.S.  Environmental Protection  Agency
  Robert S.  Kerr Environmental Research Laboratory.
  P.O.  Box 1198
  Ada,  OK  74820
                                      13. TYPE OF REPORT AND PERIOD COVERED
                                        Final  (11/27/78 - 12/31/85)
                                      14. SPONSORING AGENCY CODE
                                        EPA-600/15
 15. SUPPLEMENTARY NOTES
  Project Officers:
  Curtis C.  Harlin
Lowell E. Leach,  Jack Witherow, H. George  Keeler,  and
 16. ABSTRACT
       The Lubbock Land Treatment System Research and Demonstration Project, funded  by
  Congress in 1978 (H.R. 9375),  was  designed to address  the  various issues concerning
  the use of slow rate land application of municipal wastewater.   The project involved
  the 1)  physical expansion of an overloaded 40-year old Lubbock  slow rate land treat-
  ment system; 2) characterization of the chemical, biological  and physical conditions
  of the  ground water, soils  and crops prior to and during irrigation with secondary
  treated municipal wastewater;  3) evaluation of the health  effects associated with
  -f)ie slow rate land application of  secondary effluent and 4)  assessment of the
 'cvfects of hydraulic, nutrient and salt mass loadings  on crops, soil and percolate.
  Percolate investigations, described in this volume, evaluated the fate of
  infiltrating nutrients from applied wastewaters in the root  zone at test plots
  located on both study farms.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lDENTIFIERS/OPEN ENDED TERMS  C. COSATI Field/Group
 3. DISTRIBUTION STATEMENT


  RELEASE TO PUBLIC
                         19. SECURITY CLASS (This Report I
                          UNCLASSIFIED
21. NO. OF PAGES

   162
                         20. SECURITY CLASS (Tillspage)
                          UNCLASSIFIED
                                                    22. PRICE
EPA Form 2220-1 (9-73)

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                                           EPA/600/2-86/027b
                                           February 1986
        THE  LUBBOCK  LAND  TREATMENT SYSTEM
       RESEARCH AND DEMONSTRATION PROJECT

                    VOLUME  II

    Percolate Investigation in the Root Zone
                       by

          R.  H.  Ramsey  and  R.  M.  Sweazy
             Texas  Tech  University
              Lubbock,  Texas 79409
       EPA COOPERATIVE AGREEMENT CS806204
                Project Officers

                 Lowell  E.  Leach
                Jack L. Witherow
                H. George Keeler
                Curtis C. Harlin
          Wastewater Management Branch
  R.  S. Kerr Environmental Research Laboratory
              Ada,  Oklahoma  74820
 This  study was  conducted  in  cooperation  with:

         LCC Institute  of Water  Research
              Lubbock,  Texas 79407
       Dennis  B.  George, Project Director
ROBERT S. KERR ENVIRONMENTAL RESEARCH LABORATORY
       OFFICE OF RESEARCH AND DEVELOPMENT
      U.S. ENVIRONMENTAL PROTECTION AGENCY
              ADA, OKLAHOMA  74820

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                          DISCLAIMER
     The information in this document has been funded in part
by the  United  States  Environmental  Protection Agency  under
assistance agreement No.  CS806204 to Lubbock Christian College
Institute of Water  Research who  contracted  with Texas  Tech
University for this  research.   It  has been subjected to the
Agency's peer and administrative review and has been approved
for publication as  an  EPA  document.   Mention  of trade  names
or commercial  products  does  not   constitute  endorsement  or
recommendation for use.
                          n

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                                  FOREWORD
      The U.S.  Evironmental Protection Agency was  established  to  coordinate
 the administration of major Federal  programs designed  to  protect  the  qual-
 ity of our environment.

      An important part  of  the Agency's  effort  involves the  search  for
 information about environmental  problems,  management  techniques, and  new
 technologies through  which  optimum  use  of  the  Nation's  land   and  water
•resources- can  be assured  and  the  threat pollution poses  to the welfare  of
 the American people can  be-minimized.

      The U.S.   Environmental  Protection  Agency's   Office  of  Research  and
 Development conducts  this search  through  a nationwide network of research
 facilities.  As one of  these  facilities,  the Robert S. Kerr  Environmental
 Research Laboratory  is  responsible for the  management of programs  including
 the development and demonstration  of  soil  and other natural  systems for  the
 treatment and  management of  municipal wastewaters.

      The slow rate land  treatment  process  of  municipal  wastewaters uses  the
 unsaturated soil  profile  and  agricultural  crops  managed  as  the  treatment
 media.  The Lubbock  Land  Treatment System  Research  and Demonstration Pro-
 gram,  funded by  Congress  in 1978  (H.R. 9375)  was designed to address  the
 various issues  limiting  the  use of slow rate land  application  of  municipal
 wastewater.  The  project  involved  expansion  of the  Lubbock Land  Treatment
 System to 2,967 hectares; characterization of the  chemical, biological  and
 physical condition of  the ground water,  soils and  crops prior  to  and  during
 irrigation with secondary treated  municipal  wastewater;  and evaluation  of
 the U.S. Environmental  Protection- Agency's design  criteria  for   slow rate
 land application.   Results  demonstrate  that,  where  such  systems   are cor-
 rectly designed and  operated,  they can  be cost effective alternatives  for
 municipal  sewage  treatment at  sites where  conditions are  favorable for  low
 hydraulic loading combined with cropping practices.

      This report  contributes to the  knowledge  which  is  essential for  the
 U.S.  Environmental Protection  Agency  to meet requirements of  environmental
 laws  and enforce  pollution  control  standards  which  are  reasonable, cost
 effective and  provide  adequate  protection for the  American public.
                                     Clinton  W.  Hall,  Director
                                     Robert S.   Kerr  Environmental  Research
                                       Laboratory
                                     111

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                                 ABSTRACT
     An investigation of the amounts  and quality  of percolate generated by
the  land application of  secondary effluent from the Southeast-Water
Reclamation  Plant at Lubbock,  Texas was conducted at two sites.  One site was
located on the  Frank Gray farm (Friona Soil  Series) which had served  as a
land treatment site for four  decades.   The other site located on the Gene
Hancock farm (Amarillo Soil  Series)  near Wilson,  Texas, was receiving its
initial applications of  treated  wastewater.   Three test plots  were
constructed  at  each  site and equipped with  3 replicates  of  3  extraction tray
lysimeters  placed-under layers  of  undisturbed  soil  at 61, 122 and 183 cm
depths.  Two pairs of 76 cm diameter  tube lysimeters,  122 cm and 183 cm in
length, containing cores of undisturbed soils, were also emplaced on the plot
with their, top surface 30 cm  below the surface.  One plot at each site was
planted to  bermuda grass,  one  to grain sorghum,  and one to cotton.   The
amounts  of  treated effluent applied to the plots during the project period
were less than  the design amount.  This greatly decreased  the amount and
frequency of daily percolate collected from the lysimeters during the project
period  and  reduced the  effectiveness  of the study results.   Periodic quality
analysis was made of percolate samples.  The nutrient parameters in percolate
samples,  with the exception  of nitrate and potassium, were generally  reduced
by a factor  of  10 or more from those  of the applied water where more than one
water  quality  test for the  constituent was performed.   The  mass of cations
and anions contained in the  amounts of percolate with pH levels in a range of
7.4 to  8.8 measured in the root  zone  would adversely impact  the quality of
the ground water underlying  the  Hancock site.

     This report, covering the period from January 1,  1980 to completion on
September 30, 1984, is  submitted  in  fulfillment of EPA Grant CS806204 to
Lubbock Christian College Institute of Water Research.
                                    iv

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                              CONTENTS
Foreword	iii
Abstract	   iv
Figures	   vi
Tables	vii
Acknowledgement  	   ix
    1.  Introduction 	    1
    2.  Conclusions	 .    3
    3.  Recommendations  	    5
   • 4.  Research Approach	    6
           Site Characteristics  	    6
           System Design and Monitoring Procedures 	   10
    5.  System Operations  	   41
           Lysimeters	   41
           Irrigation	   44
    6.  Results and Discussion	   48
           Percolate Collection Activities 	   52
           Soil Analysis	   70
           Field Use of Extraction Lysimeters	   85
References	   88
Appendices
    A.  Profiles of Test Soils	   91
    B.  Hydraulic Loading Rates	 . .   94
    C.  Nitrogen Loadings  	  101
    D.  Percolate Quality Parameters at the Test Plots ....  105
    E.  Equivalent Ratios for Water Charateristics ......  137
    F.  Mass Inputs in Applied Wastewater and Mass Outputs in
            Percolate and Crops Harvested  	  144

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                                   FIGURES

Number                                                                   Page

 1     Location of the Hancock Farm Test Site	   7
 2     Location of the Gray Farm Test Site	8
 3     Plan of Test Facility	11
 4     Arrangement of Percolate Collection Units in Tube Lysimeter ....  13
 5     Extraction Tray Design	  .  16
 6     Wick Assembly	18
 7     Lysimeter Control  Panel Design  	  20
 8     Irrigation Coverage of Test Plots at the Gray Site	28
 9     Irrigation Coverage of Test Plots at the Hancock Site .  	  29
                                      Vf

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                                   TABLES

Number                             -                                       Page
 1     Seasonal Water and Nutrient Use by Crop Types Utilized
          in Study .	9
 2     Precipitation  Values for 5-Year Return Period 	  :  ...  21
 3     Monthly ET  and ET     Values  for Conditions at Lubbock,  Texas.  .  .  23
                 p       crop
 4     Weekly Irrigation Schedule  	  27
 5     Measurement Frequency of Weather Parameters 	  32
 6     Water Analysis  	 	.34
.7     Sampling Schedule for Percolate 	  35
 8     Sampling Schedule for May 1983 to August 1983	36
 9     Soil Analyses	38
10     Crop Analyses	39
11     Hydrologic Factors at the Gray Site for 1982	53
12     Hydrologic Factors at the Hancock Site for 1982	54
13     Hydrologic Factors at the Gray Site for
          January 1 to September 30,  1983	  55
14     Hydrologic Factors at the Hancock Site for
          January 1 to September 30,  1983	  56
15     Monthly Percolate Data in mm for the Bermuda Grass Plot
          at the Gray Site from October 1982 to September 1983	60
16     Depth of Percolate Intercepted by Lysimeter Units Over
          Study Period at the Hancock Site	62
17     Depth of Percolate Intercepted by Lysimeter Units Over
          Study Period at the Gray Site	63
18     Percolate and  Water Quality Samping Events from
          May 1, 1982 to September 30, 1983	  64
19     Crop Yields and Geometric Means of Selected Parameters
          for Test Crops Grown in 1982	66
20     Crop Yields and Geometric Means of Selected Parameters
          for Test Crops Grown in 1983	67

                                     vii

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21     Geometric Means of Concentrations for Quality Parameters in
          Irrigation Waters Applied to the Test Areas over the
          Project Period .	,	68
                      r\
22     Changes in 10~£Mg/g of Soil with Depth for Selected Cations
          and Anions Between Sampling Periods in
          March 1981 and November 1983	72

23  -   Results of Soil Analysis for TKN-N on Test Plots
          for 3 Sampling Periods in 10~1 mg/g of Soil  	 ..... 73

24     Results of Soil Analysis for N03  -N on Test Plots
          for 3 Sampling Periods in 10~^ mg/g of Soil	74

25     Results of Soil Analysis for NH3  -N on Test Plots
          for 3 Sampling Periods in 10"^ mg/g of Soil  ..... 	 75

26     Results of Soil Analysis for Total Phosphorus-P on Test Plots
          for 3 Sampling Periods in 10"! mg/g of Soil	76

27     Results of Soil Analysis for Orthophosphate-P on Test Plots
          for 3 Sampling Periods in 10" 3 mg/g of Soil	78

28     Maximum Concentration in PPB and Location of Organics
          in the Soil Profile at the Test Sites in November 1983 . ... . .79

29     Application of Metals in Wastewaters and Fate of Metals
          in Plot Root Zone over Project Period—Gray Site	81

30     Application of Metals in Wastewaters and Fate of Metals
          in'.Plot Root Zone over Project Period—Hancock Site  ...... 82

31     Bromide Tracer Location in Plot Soils in March 1983
          After Application in May 1982	83

32     Bromide Tracer Location in Plot Soils in November 1983
          After Application in May 1983  . .	84
                                    ym

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                                ACKNOWLEDGEMENT
     This report  was  prepared-under a  contract  with the  Lubbock  Christian
College Institute of Water Research  with funds provided by EPA Grant  CS806204.
The authors would like to acknowledge the help  and  cooperation  of  the  Institute
staff in the performance of the project  activities.
                                       IX

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                                SECTION I

                               INTRODUCTION
     Since  1939, the Frank Gray  farm,  located east of  Lubbock,  Texas, had
served as a land  application site for the city's  treated wastewater.   During
the seventies,  this facility  experienced difficulties  in  handling the
additional  wastewater that had been generated by  the growth of the city.  The
hydraulic  loading  rates  used  on  the farm were in  excess of the rates
recommended for slow rate systems  by  both the EPA and  the State  of Texas.  A
new land  application site north  of Wilson, Texas,  was developed to reduce the
loadings  being experienced at the  Frank Gray farm.

     In conjunction with the construction of  the  new site,  a research  effort
was initiated to  evaluate the effects of the  soil-crop matrix"on the  quality
and quantity of the applied wastewaters percolating through the soil normally
penetrated by  the roots of field crops.   These upper soil  layers,  known
collectively as  the soil root zone, possess   physical,  chemical,  and
biological  characteristics that  affect the agricultural productivity of the
site.

     Successful implementation  of land application systems  for municipal
wastewater  treatment is predicated on  the effective removal and stabilization
of wastewater  constituents in the  soil  profile.  Monitoring of the ground
water under and adjacent to the  site  is necessary to  insure  that the land
application system is functioning  as intended.  Evaluating the percolate
quantity  and quality as it leaves  the  root zone should provide information on
potential  detrimental conditions that would enable changes  to  be made  in the
operational procedures of the  land  application  system  to  lessen pollutional
impacts on  the underlying ground water.  A current problem associated with
the monitoring  of ground water under and adjacent to land application sites
is that  by the  time poor quality conditions  are noted  in  ground  water,
corrections in  the system's operation will have little short-term effect
because  of the  mass of pollutants  already in  transit through the soil
profile.   The  uncertainties associated with ground water movement under the
test  sites, a  depth to ground water ranging   from  3.0  to 27.4  m,  and
variations in  the physical properties of the soil  profile  could cause
problems  in monitoring .short-term  effects of the  land application systems on
the ground  water under the two sites used by the  City of Lubbock.

     The  study devised for the  investigation  of impacts resulting from
physical,  chemical,  and biological  activities in the soil  root zone on
percolate  flow  and quality had  two objectives.  As stated in the original
proposal, these were:

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     (1)   To obtain information on  the  amount and rate of water  movement in
          the  unsaturated  zone under  different cropping management  systems;
          and

     (2)   To obtain data on the quality of water applied to  the soil  and that
          drawn from different soil  depths in the unsaturated  zone.

     To accomplish these objectives,  test facilities were constructed at the
Gray and  Hancock sites.  The test facility on the Gray site  was located  in
an area adjusting to a lower hydraulic loading  while the  test  area at the-
Hancock site  was constructed  in  an area just being subjected to irrigation
with treated wastewater.

     Measurements were made of the  precipitation  and of irrigation waters
applied to three .cropping  systems that were of economic  importance to the
region  and which  exhibited a  range of water and nutrient requirements during
growth.   The  crops grown  on each test facility site were cotton,  grain
sorghum, and bermuda grass.

     Considerable biological and chemical activity occurs in the  near-surface
zone .among the life forms inhabiting the soil  and the various  and  complex
soil,  soil-water,  and soil-atmosphere interfaces present.   To  monitor
percolate flow  and  possible  quality  changes with  soil depth,  lysimeter
systems were installed so that percolate could be obtained at  three different
levels  in  the root zone under each  test plot.

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                                SECTION II

                                CONCLUSIONS
1.    The extraction lysimeters utilized in the study are  not suitable for use
as  monitoring devices in operational  land treatment systems primarily because
of the  high  costs associated  with  their installation and  operation when
compared to conventional ground water monitoring.

2.    Hydraulic  loading  rates  utilized during  this  study  were  insufficient to
produce  percolate for quantity  and quality analysis for use  in evaluating
current  design criteria for test crop conditions  using  slow-rate  land
application procedures.

3.    The inability to apply design  hydraulic loadings to the test plots, to
intercept percolate in  the soil profile, and to accurately  measure
evapotranspiration on the  test  plots caused  unexplained  losses  of such
magnitude that  accurate and meaningful water or solute balance determinations
for the substances measured during the project can not be developed.

4.    The lysimeter techniques utilized in the  project cannot reproduce the
conditions of soils in their natural  state nor detect the subtleties inherent
in  the  hydraulic responses of undisturbed soils at a specific  locale.

5.    The mass of  cations and anions  contained  in  the small amounts of
percolate at pH levels in a range  from 7.4 to 8.8 measured in the root zone
of  the  test plots irrigated with wastewater effluent may  adversely impact the
quality  of the ground water underlying the Hancock site if  irrigation with
wastewater effluent is continued at design rates over a period of years.

6.    Except for nitrates and potassium, the nutrient parameters, in percolate
collected from  lysimeters where more than one  water quality  test  for the
parameter was  performed, were generally reduced by a  factor  of 10 or more
from the applied water.

7.    Test facilities utilized on the  project were subjected  to  flood  damage
and operational  delays as  a result of piping actions caused by fissures in
the soil  profile.

8.    Experiences in this  study indicated that  better  techniques  must be
developed to  measure and  adjust vacuum  levels employed in extraction
lysimeters.

9.    From an  operational  basis, slow-rate land application systems utilizing
forage  crops offer less conflicting  interactions among weather  factors, crop

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cultural needs,  farm machinery use,  and wastewater irrigation schedules than
other crops.

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                                SECTION III

                              RECOMMENDATIONS
1.    A long-term study would be essential  to determine  the influence of crop
production  and biological  activities in the root zo'ne on  the flow patterns
and quality  of  percolate generated  by the land application  of municipal
wastewater.

2.    The  area! occurrence,  frequency of flow events, and magnitude of  the
mass of  water-borne solutes and  pathogens transported  through macropores in
the soil  matrix  should be investigated at land application sites.  When
ponding  of wastewaters on  the surface occurred, macropores  flowed  under
hydrostatic pressure.

3.    Appropriate tracer materials should be added to  irrigation water in
order that the  rates of water and  solute movement can  be determined  under
different rates of hydraulic  loading.

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                                 SECTION  IV

                             RESEARCH APPROACH
SITE CHARACTERISTICS
     The selection of the test  areas on the  Hancock  and  Gray farms  was
originally predicated  on  the soil characteristics  of  the  facilities, past
management  practices.,  and surface drainage.

Hancock Site

     Because of the locations preempted for  center pivot irrigation  units,
the test sites  available for selection  on the Hancock  farm were restricted to
corner areas.   The  site chosen is indicated  in Figure  1.

     In previous years, when ground  water  had  been available  for furrow
irrigation,  the row orientation was from north to south.   The test  plots
occupied the head  row area  that  had  existed  during the early irrigation era.
This could  imply that  greater amounts of irrigation water had percolated down
through the soil profile of the test area than in  those areas located further
down slope.

     Site location  had impacts on both  the availability and quality of water
used during project  activities.  The  distribution  system  installed on the
site could not be  designed  for maximum flexibility of  operations.   The
location of the test area on the farm prescribed that the water supply line
be connected to an  0.38 m diameter pipeline  on the eastern boundary  of  the
site.   This pipeline was  the  primary transmission line for conveying treated
wastewater  from Lubbock to a 1.48 x 106 m3 storage lagoon.   The irrigation
water applied at the test  site was  generally  water that  had  been pumped from
Lubbock rather  than water from the storage lagoon.

Gray Site

     The test facility at the Gray site was  selected  from among the  field
areas  which had the  longest histories of  treated effluent  irrigation.  The
location of the facility is shown in Figure 2.   The ditches adjacent to these
roads prevented highway runoff from entering  the plot  area.   The land  slope
of the  test area was from  east to west at less than 1 percent.  The field
plots were  supplied with irrigation water from a wastewater effluent  storage
lagoon located  approximately 1.5 km northwest of the site.

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Figure 1.   Location of the Hancock Farm Test Site

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Figure 2.  Location of the Gray Farm Test Site
                        8

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Plot Layout

     The crop systems  selected for both test areas were  cotton, grain sorghum
and bermuda grass.   These crops were of economic importance  in the region and
also exhibit varied  ranges of water and nutrient requirements during growth
(Table 1).   Only one plot for each crop was planned at each  test area.

     Three  adjoining  0.84 ha  plots (91.5  m  per side)  were laid  out and
enclosed  by a cyclone  fence.  The percolate collection facility was located
at the center of each  plot.  The  45-m  distance  from the plot boundary to the
test facility was  assumed to be sufficient to  eliminate boundary effects
caused by other land uses on areas adjacent to the test  plots (15).

Soil Characterization

     The test areas  at the  Gray and Hancock farms  were  located on  the soil
types that the county  soil  survey publications  for Lubbock  and Lynn counties
(3, 12) showed to comprise  the largest acreage on  the farm.  The Gray test
area was  located on  a  soil  of the Friona series and the Hancock area was
located on one of the Amarillo  series.   Both are  loamy soils located on
uplands  and formed in  calcareous, loamy eolian deposits.  Typical profile
descriptions of the  soil are provided in Appendix  A.


                                  TABLE 1

                     SEASONAL  WATER  AND NUTRIENT USE BY
                        CROP  TYPES UTILIZED  IN STUDY




Crop
Bermuda grass0
Cotton
Grain Sorghum
Total
consumptive
use of
water3
(cm)
102d
76
46


Nitrogen
(kg/ha)
400-675
75-110
135

Nutrients ,
phosphorous
(kg/ha)
35-45
15
15


Potash
(kg/ha)
225
40
70
?Hansen et al.  (18).
process Design Manual Land Treatment of Municipal  Wastewater  (18),
 .Nutrient figures  are for coastal bermuda grass.
 Water use figures are for pastures.

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SYSTEM DESIGN AND  MONITORING PROCEDURES

Lysimeter Systems  Design

     Two types of  nonweighing lysimeters using undisturbed soil profiles  were
installed on the test plots.  The first type, hereafter  referred to as  tube
lysimeters, consists of  a form made  of  appropriate  siding material  to be
pushed  down through the  soil  profile  at  the  sampling site (4).   After
reaching the appropriate depth, the  form with its encased soil core  is
removed.  After equipping the unit with a percolate collection system,  the
enclosed soil core is  used as the  test  material.  The  test unit can  be
installed in the laboratory or at a  field  site.  The  other type involved
employs trays filled with  a disturbed soil to  capture  soil percolate;  these
are placed under,  and in contact with, the  overlying, undisturbed soil  profile
by means of horizontal excavations (7).   The tray technique is site specific.

     Vacuum devices were used to obtain percolate from the  lysimeters.   The
vacuum  level was  adjusted  to the level measured by a tensiometer located in
adjacent undisturbed soil.  If soil  characteristics were  uniform,  this
practice would insure that the area of influence  on moisture transport in the
profile above the tray or  tube is no greater or less than a comparable  area
in .the undisturbed profile.

     Replicates of the two lysimeter techniques  for collecting soil percolate
were  utilized on  each test plot.   Three  trays,  located  in cavities  108
degrees apart, were placed at depths of 61, 122, and 183 cm.  Pairs  of  tube
lysimeters were emplaced with the upper surfaces 30 cm  underground so  that
normal  tillage operations  could be conducted.   Percolate was collected  from
one pair of tube lysimeters  at a depth of 122 cm  and from the other pair  at
183 cm.   One plot  on each farm area had an  additional pair of tube lysimeters
which collected percolate at the 244 cm depth.

     An underground  chamber containing the necessary  support equipment for
the installed vacuum extractors was  installed  at the  center of each  test
plot.   The lysimeters were placed in the soil radially around the chamber and
at distances far  enough from it so as not to be influenced by the chamber's
interference with  soil percolate flow.  The  use of a circular chamber  allowed
the units to be placed within a  small  area, thus minimizing both differences
in soil  characteristics and  in plot size.   A plan view  of a test facility is
shown in Figure 3.  A detailed description  of the units, their installation,
the supporting facilities,  and operational  characteristics follows.

Tube Lysimeters—
     The tube  lysimeters  were  constructed from used  76.2 cm 00 steel  pipe
with a wall thickness of 0.95 cm.  The  soil area within pipe sections was
0.434 ma.   The number and  length of  the  tube lysimeters installed on the
project were:   14  with a length of 107 cm,  14 with  a length  of 168 cm, and 4
with a length of 229 cm.

     Three  angle  iron  ears were  welded at points 120 degrees apart on the
pipe  surface at  about 30  cm  from the  top of  the pipe.  These served as
attachment points  for chains used  for either lifting or positioning the  pipe

                                    10

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    Vacuum Pump

        Manhole
Sample Collection
     Units
  Tensiometers
                                                    Extraction Tray
                                                    1.52m x .15m
                                                    (3  Trays will be emplaced at
                                                    each of the 3 specified depths)
                                                                     Tube Lysimeters
                                                                     2 - 1.07m-Length
                                                                     2 - 1.68m Length
                                                                     Buried 0.3m below surface
                                 Figure 3.  Plan of Test Facility

-------
sections.   The pipe  sections were taken to the test  area and placed at points
that had been randomly selected on the plot map around the proposed locations
of the percolate  extraction facilities.   Each point on  the surface  at  the
site was  assumed to overlie material  of the same soil type and to exhibit
uniform profile conditions.  The processed units from  each farm area were
later  indiscriminately assigned to one of the three test facilities at each
site.

     At the designated location, the top 30 cm of soil  was  scraped off  and
the pipe  section was placed vertically on this surface then driven into the
soil under, existing  site conditions.  Water was not  applied  to wet the  soil
material.   Only in very  few instances  did  the p'ipe  advance  exceed 2.5 cm per
blow.   Generally,  the penetration was  1/20 to  1/5 of this value.   Excavation
of the  soil  around the outside of the pipe after  driving  the pipe into the
ground a few centimeters was found to increase the depth per blow.  After the
pipe sections had been driven to their final  depth,  the units were lifted  and
loaded for transport to a processing area.

     In the processing area, each pipe section was inverted,  exposing  the
bottom  of the soil profile for further processing  (Figure  4).  The lower 15
cm of soil in the original profile was removed and two percolate extraction
units were installed so  that, if failure  in one unit occurred, percolate
collection from the  lysimeter continued  through the remaining unit.  Each
unit utilized three  porous ceramic,  round-bottomed,  straight-wall  cups, rated
at 1 bar under high flow conditions;  these were 4 cm in diameter by 19 cm in
length.  . The cups were connected tpgether with tygon vacuum  tubing having 6
mm I.D.  and 4.8  mm wall thickness.  The cup connection to  the vacuum tubing
consisted of a short length of glass  tubing  which  passed  through a  rubber
stopper cemented in the  end of the  cup,  and was inserted into the vacuum
tubing.   The vacuum  tubes  for each  unit  passed through a hole constructed in
the side of the lysimeter.  Rubber grommets were fitted around the tubing  and
coated with silicone sealer to provide an effective  water barrier.

     At this time,  a control  ten-siometer,  consisting of a porous  ceramic  cup
with a suction value of 1 bar, cemented and sealed with cold-setting silicone
rubber to tygon tubing was installed.   The tubing (11 mm I.D. and  1.6 mm wall
thickness) for this unit  also passed  through a  grommetted  hole  (19  mm
diameter)  in the side of  the  lysimeter.   After inspection, the soil taken
from the bottom of the lysimeter was replaced and packed  by  hand  around  the
extraction units.  The remaining void was then  filled with soil that had
originally been taken from the unit.   A  bottom plate was placed on this
surface and tack-welded to  the  pipe.   The  pipe section was  then inverted  and
the bottom plate  was welded to the pipe  section.    The welded  joint,  after
cleaning and  inspection,  was sealed  with a  coating of silicone.

     The prepared  tubes were transported to the test facilities where a crane
was used  to place  each lysimeter on earth footings that had been leveled to
the proper depth in the  excavation.   Tygon vacuum tubing was laid in a
prepared  trench  from the test facility to each lysimeter and connected by a
polyethylene  male-female connection to the short piece of  tubing that  had
been  provided on  each extraction unit.   The connections  were cemented
together and  sealed  with a cold setting silicone rubber.  Tygon tubing from

                                    12

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           4cm Dia Ceramic Cup
           for Percolate Collection
Tensiometer
   Unit
                                                   15 cm
Tygon4*.
Tubing
for
Percolate
Collection
                                                Collection Plane
                        ,76m Diameter
                             x
                        1.07m Height
      Figure 4.  Arrangement of  Percolate Collection
                 Units  in Tube Lysimeter
                            13

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the test manhole was  connected to  the control tensiometer at this time also.
After inspection of all connections, the  tube lysimeters  were buried with
material excavated from the lysimeter trench.  Stored topsoil was then  spread
over the tops  of the  tube lysimeters to  a  depth of 30 cm.

     Soil  compaction did  occur during the process  of  driving the pipe
sections into  the soil profile.  Excavation of the bottom 15 cm of soil  from
the unit was difficult in  all  cases,  indicating that the density of the soil
in the lysimeter may  have  been greater than that observed and experienced  at
adjacent depths outside of the driven pipe sections.  Two permeability tests
using a falling head  permeameter with no pressure were  conducted on soil
samples taken  from the bottom  of two units.   Results gave rates  of
permeability below 1  x 10"8 cm/sec.  These results and  the packing  of the
soil that .was  evident in the removal of  the lower  15 cm of soil from the test
units  caused  concern about  the validity of comparisons between percolate
flows in field soils  and those found within the tube lysimeters.

Tray Lysimeters—
     The design  and  installation of the tray lysimeters  utilized  in the
project  were  based  upon  the extraction  devices  developed by Duke and Raise
(6).  The 56 trays used on the project were 15 cm wide,  20  cm deep, and 150
cm  long.   The top area of  each tray was 0.232 m2.  Four trays utilized for
extracting  percolate  samples  for priority  organic  analysis  were constructed
of  stainless  steel (fittings and tubing  were constructed from  teflon
material) whereas the others  were constructed  of 18-gauge  galvanized  sheet
metal.

     The tray lysimeters were installed  in  horizontal cavities dug radially
outward from the plot's underground equipment shelter.   A plan view is shown
in Figure 3.  The underground  equipment shelter (manhole) was constructed  in
an excavation  that had been obtained by boring a 3.35 m diameter hole  at the
center  of  the test  plot to a depth of  3.35 to 3.65 m.  The placement  of the
boring rig  and,  subsequently, the travel  of other vehicles on the test plot,
were restricted to  the sector  where a  later  excavation was to be made  to
place the tube lysimeters.  The side walls of the manhole were formed  into a
10-sided polygon,  3.2 m  in  diameter and  2.8  m  high.  Treated tongue-and-
groove'lumber,  5 cm  thick,  was  bolted to three angle-iron "hoops."  The
exterior corner joints on each side were covered with a strip of 20.3 cm-wide
galvanized  flashing material.   The completed,  painted wall units were'lowered
into the prepared excavation.

     After  leveling the wall  sections, rectangular openings, 25 x 30 cm, were
cut  into  the wooden walls  at each tray lysimeter  location so that the
rectangular cavity could be drilled for installing the  tray.   Once the holes
were cut,  metal flashing was placed around the rectangular openings to hold
back pea gravel  poured to fill the void space  between the soil and the  wooden
wall.   The gravel  provided  a  rapid drainage  pathway for  the  percolate
intercepted by the manhole roof.   It was  found that a grouting operation was
necessary to stabilize the pea gravel  around the rectangular cavities.

     The hydraulic soil coring and sampling machine that  had been modified
and used by Dukes at Colorado  State was employed to dig  the horizontal

                                    14

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cavity.   The  horizontal cavities  for the trays  were dug in two  steps.   A
10 cm diameter pilot hole was drilled with a flight auger  to a distance of
2.5 to 3 m  horizontally into the earthen wall.  Loss of control in  vertical
alignment of  the pilot hole caused  a  dome to form in the final cavity roof in
the first  four holes drilled.   These holes were modified by redrilling and
increasing  the cavity length  until  a flat  section was available for the
1.52  m tray.   Stabilization of the boring  unit so that horizontal and
vertical alignment was maintained during construction of the cavity was
essential.

     After completion  of the  pilot  hole, a rectangular coring device with a
sharp front edge that sheared  the soil to produce the final rectangular-
shaped  cavity was pushed  into the  soil by hydraulic pressure.  The sheared
soil  was stored in the interior  of the coring  device.  A portion of  soil
removed  during the coring phase  was placed in plastic garbage bags and used
to fill  the tray installed in that particular  cavity.  The three  holes at
each  depth  were drilled 108 degrees apart to provide as large a sampling area
as possible.

     Holes were punched  in the  end  of the tray nearest to the manhole.  The
hole  location and dimensions are shown  in Figure  5.   An inflatable air bag
was constructed for each  tray.   The  inflated  air bag was to  keep the tray in
contact with  the roof of the cavity in a manner similar .to that used  in the
Colorado State  study.   Lay-flat butyl  tubing,  10 cm in diameter, was cut into
1.5m segments to form  the air  bag.   A valve  stem from a truck tire was
attached by vulcanization to each  segment.  The  ends  of each bag were folded
and sealed  by vulcanization. An air  bag was then glued to the bottom of each
tray.   An  airhose assembly,  that had been previously checked for leaks by
submersion in a  water bath while attached to  an  inflated bag,  was  then
connected  to the  valve stem and  the air bag was inflated.   Air pressure was
maintained  for  at least a week  for leak detection.   The air  bag assembly was
then deflated and remained in the  deflated state until  after the tray had
been  inserted into the cavity.

     The extraction units consisted of five ceramic tubes fastened  together.
These tubes were made by  sawing off  the closed ends of flat-bottom  straight-
wall  porous  ceramic cups  30  cm  in  length;  they  had a  one bar  bubbling
pressure.  The modified cups  were joined by cementing a tygon tubing sleeve
to two adjacent units.  One end  of each complete  unit was connected  to a
plastic  fitting  that passed through the end of the tray during installation
and was  joined to a length of tygon vacuum tubing  during the installation
process.   The vacuum tubing from the two extraction units in the tray would
be joined  to a Y-connection  located in the manhole which provided  two
separate percolation collection  systems.  If one extraction unit  failed it
could be sealed off and the other  used.

     The other end of the extraction  unit was fitted to a length of  3 mm-I.D.
tygon tubing.  During installation  this piece of tygon tubing was folded back
and buried  in the fill soil  of  the tray.   The  remainder of the tubing was
passed through  a separate hole in  the end of  the tray closest to the manhole
and was  terminated in the  manhole.   The ends  of  the tubing were tightly
crimped  to  prevent air entry.   This small tube could be used  to flush out the

                                    15

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                          Sheet Metal Ties
                          38cm O.C.
                          Riveted or Spot
                          Welded to  Sldewalla.
Fabricated from 18 ga
Galvanized Steel
          20.3 cm
16 ga Ties Recessed approx
'1.2 cm below top of Trough
m
•m
m
m
m


-
1 1
1 .--l^ cm
i T
_L^-6 ™M_
-
-------
ceramic tubes  if a slime buildup were to occur.  The wick  assembly is shown
in Figure  6.

     The  installation of  each  tray lysimeter  began with the placement of
sifted soil  (wire mesh with 1 cm between strands) in the bottom of the tray
to a depth of 2 to 2.5 cm.  Two wick  units were placed on  the  soil bed in the
bottom of  the tray.  The  tygon tubing and  plastic fittings were  inserted
through the proper holes then sealed  with grommets in the  end  of the tray.  A
coating of silicone sealer was  placed over each grommet both on the inside
and outside of the tray.  Soil  was then gently placed around and  over the
ceramic candle.   The remaining space in the tray was filled  by placing thin
layers of sifted soil in  the tray  and firming  these layers by  hand.   A
tensiometer unit consisting  of  a porous  ceramic cup glued to a  length of
tygon tubing sufficient to  reach the manhole cavity was installed just below
the soil  surface  in the tray.

     After filling  and leveling  the  soil  in  the tray, a thin layer of soil
was sifted over the tray.   The  tray was then moved from the  assembly point to
the entrance of its  respective cavity and  pushed into the cavity beneath the
undisturbed soil  zone.  After  the  lengths  of vacuum tubing  were glued to the
plastic fittings  and coated with silicone  sealer,  the tray was pushed to its
permanent  position.

     When all the  trays  had  been installed,  the air bags were inflated to
raise the  trays to positions where they were in contact with the roofs of the
cavities.   About  half the bags  deflated within 24 hours.  The 75  to  80 kg
weight of some  0.045 m3 of soil  in the tray  imposed greater stress on the
inflated  bags than had been experienced in  the pre-i nstal lation  leak  test
under  no-load  conditions.  Rather  than repair the air bags,  a decision was
made to place wooden wedges under each tray.   Three pairs  of wedges  were
forced into position between the sides of the cavity and the inflatable bag.

     After installation  of the tray lysimeters, the manhole  structures were
completed.   Each unit was  floored  and a  sump  pump  was  installed'  in  a
reservoir under  the floor.   The outfall  of  the sump pump was a gravel bed
buried at  a depth of 60 cm below the  soil surface  and located 6 m  from the
edge of the manhole.   An earth-covered roof was constructed  over each unit.
Access to  the unit was by means of a  manhole 1  m in diameter.  An  air  vent
system was  installed to produce" an air circulation pattern that reduced
humidity  levels in the manhole  facility.

Vacuum System—
     The  lysimeters in each battery were in close proximity  and the number of
units in each battery ranged from  13  to 17.  A vacuum system  similar  to the
system employed  by Dr.  Harold  Dukes of Colorado State University (7), was
used in this study.  The  volume of space in  the wick  system and  the
connecting  vacuum tubing  lines  was estimated for the respective  lysimeter
batteries  to determine the volume  evacuated.  One vacuum unit  with a 38 liter
reservoir  serviced the lysimeters  in  each battery.

     The  lysimeters were attached  individually to the vacuum  unit  through  a
loop system.   Each lysimeter unit  had an individual control panel.  This

                                    17

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                           Tygon Tubing
                           11 nun ID
                           14mm OD
                           3cm Length
                           Bonded with CPVC Cement
      Ceramic Candle
      10mm  ID
      13mm  OO
      300mm Length
           Tygon Tubing
           7.9mm ID
           18  mm OD
        /
00
                 Polyethelyne
              To
           Access Well
Plastic Pipe
10mm ID
13mm OD-_
ne /
nnector1 /
1
-1 U
f

!
	 i
i 	

1
n L


.u
1

i —
3.2mm|{l/8"
	 1
Tygon Tubing
llmm ID
14mm OD
3cm Length
           Tygon Tubing
           3.2mm ID
           6.4mm OD
           Flush Line-
                                                                                     - 27  NPT)
Ceramic Candle
10mm ID
13mm OD
300mm Length
Tygon Tubing
11 mm ID
14mm OD
3cm Length
                                                                                                 NPT x  1/4'
                                                                                                Imperial
                                         Figure  6.   Wick  Assembly

-------
system adequately handled the wide range of vacuum requirements experienced
among the  lysimeters in each battery.

     The  design for  the  control  panel utilized  for each tray or  tube
lysimeter  has  been outlined in previous  studies  (6, 7). . A schematic diagram
of the vacuum  system control panel  used'on each  lysimeter is  shown in Figure
7.

     In the  original design, the control  of the  vacuum in each lysimeter was
regulated  by using the  readings taken on two tensiometers.  One of these was
a reference  tensiometer located in the undisturbed soil  and  the other was  a
tensiometer installed in  the  lysimeter.  The.tensiometers were installed
horizontally from the manhole so that less equipment would be present on the
soil  surface.

     A reference tensiometer,  consisting of a porous  ceramic cup glued  to  a
section of  thin-wall  tygon tubing  was placed  in  the  undisturbed  soil
approximately 30 to 60 cm to  the  side of the tube  or  tray  lysimeter.   The
water reservoir for the tensiometer was also connected to a manometer in
which air  was  the fluid between the mercury in the manometer and the water in
the reservoir.

     The tensiometer  in  the lysimeter was implanted  in the  top of the  tray
lysimeter when  the tray was  being  filled with  soil and  the tubing  was
extended  through the end  of  the tray.   In the case  of  the tube lysimeters,
the tensiometer unit was installed in the bottom of the tube at the same  time
the percolate  collection units were installed.   The  tubing from the  tray
and/or  tubes  was also connected to water reservoirs consisting of plastic
pipe.  These units were hooked to mercury manometers  in  the same manner as
the reference  tensiometers.

     Originally, the first step in the lysimeter operational procedure was to
adjust the needle valve on  the control  panel  to  regulate the  vacuum level in
the candle so  that eventually the tray tensiometer manometer reading would
equal that of  the reference unit in the undisturbed soil.  A series of needle
valve  adjustments  over time  would  be  necessary to  bring  about agreement
between the  reference tensiometer and the tensiometer  in the tray or tube.
Under  the planned  schedule of irrigation, divergence in  the tensiometer
readings  was  not expected since the  moisture  content of the  soil   was
anticipated  to remain at or near field capacity during  the projected period.

Irrigation System Design

     Treated  municipal  wastewaters were to be applied  to the test plots by
sprinkler  irrigation.  The hydraulic  loading rates for  the project cropping
system were  developed in  accordance with  the recommended EPA design
procedures (18).

Hydraulic  Loading Rates—
     The design rates for a land application system may be dependent on one
or a  combination of soil  characteristics at  the site,  concentration of
materials  in the wastewater, and/or climatic conditions.

                                    19

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                                                                                        Pressure
                                                                                         Switch
ro
O
                         Tygon
                         Vacuum
                        -Tubing
                                                          Solenoid
                                                                                         1/8"  F,  l/4m
                                                                                           Bushing
V
                          Tee 6462-20
\
-Needle
 Valve
                                            Male
                                            Pipe
                                            Adapter
                                                                                                            To
                                                                                                        Extractor
^-Needle  V-i /a» no<]
            1/8
            Pipe Nipple
                        1/8"
                      NPT Tee
                                       Figure 7.   Lysimeter  Control  Panel  Design

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     Climatic factors — the following discussion  presents  the development of
precipitation and  evapotranspiration conditions  required for calculations.

     Precipitation — Forty years  of monthly precipitation data obtained at
Lubbock were used  to  determine monthly design values  for use in  the  EPA
procedure.   The National  Weather Service  recording  station at the Lubbock
International Airport  was approximately 12 km NW of  the test plot at the Gray
site and 33.8 km NNW  of  the  Hancock  site  in  Lynn County.  Frequency analysis
was employed to determine  the  monthly  precipitation- that will  occur at least
once in a five-year period.  The recurrence interval (R.I.) was calculated by
the formula:
                       R.I.
           where  l\!  =  number of monthly values,  and
                 M  =  rank of individual value.

     The monthly values  obtained  using  the analysis  outlined in  the  EPA
manual are shown  in Table 2.
                                  TABLE 2

               PRECIPITATION VALUES  FOR 5-YEAR RETURN PERIOD

Month
January
February
March
Apri 1
May
June
July
August
September
October
November
December
TOTAL
cm
1.96
2.95
4.11
4.76 '
10.11
10.85
9.53
9.27
10.44
8.76
2.74
2.60
78.08
     Evapotranspiration rates—The calculation  of  specific evapotranspira-
tion rates consisted  of two tasks.   The  first task  was  to calculate  the
potential  evapotranspiration rate.  This  value is representative of a well-
watered crop of alfalfa which is under no moisture stress  (9).  The  second
task was  to determine  the  water needs of  the crops, consisting of bermuda
grass and  annual  crops of cotton, grain sorghum and winter wheat,  to be used

                                    21

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on the test  plots during their growth and development.

     Potential evapotranspiration rates  used in determining the hydraulic
rates  for the test plots were  estimated by  means of  the Jensen-Haise
procedure (9).  This procedure,  classified as  a "radiation  method," utilizes
local temperature and percentage  of  sunshine.

     The  basic  equation  for calculating  the  potential   daily
evapotranspiration (ET  )  in langleys/day as defined for a well-watered
alfalfa crop is:        P

                       ETp = CT  (T  - Tx) Rs                   '          (2)

          where T = average monthly temperature in °C.

The other factors  in equation  (2) are variables developed from the following
equations.   Cj is a temperature coefficient defined as:

                        T = f 4- r  r   '                                 ^  '
                        I   L1 + 02LH


          where GI = 20 - [(2°C)(elevation in m above  MSL)/305],

                Cp = 7.6°C,  and

                CM = 50

The values  ez  and el  are the saturation vapor pressure in  millibars  (mb) at
the mean maximum and mean minimum temperatures for the  warmest month  at the
site.

     T  is a constant defined as:
      A

                TX = -2.5 - 0.14 (e2-e.,)0C/mb-(elevation

                       in m above MSL)/550                              (4)

     R ,  the incoming solar radiation,  is defined to be:

                RS = (0.35 + 0.61S)R$o                                  (5)

          where S = ratio of actual to possible sunshine, and

                R   = average cloudless-day solar radiation  for the month

                      in question and the latitude position  of the site.

     The average monthly temperature, percentage of  possible sunshine, and
temperature values  for  determining e:  and  e2  were obtained  from  a
climatological  summary for Lubbock published by the National  Weather Service.
The latitude and  elevation  of  the Lubbock International Airport weather
station were used rather than those  at the individual sites  since the maximum

                                   22

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difference in latitude  between the station and the sites  was  approximately 18
minutes and the elevation difference was less than 65 m.   The conversion of
langleys/day to mm/d  of  water was based upon the change  of enthalpy at the
average monthly temperature.  The monthly values of ET are given in Table 3.

     To adjust  the  potential evapotranspiration  requirements which  were
calculated for alfalfa  to evaporation  requirements for  crops grown on the
site,  crop coefficient  (kc) values were developed.   The  procedure  utilized
for determining the kc values  is that outlined in Guidelines for Predicting
Crop Hater Requirements, published by the Food and Agricultural Organization
(FAO)  of  the United Nations (5).  The monthly ETp values  were multiplied by
the appropriate kc  values to determine the monthly values for each particular
crop.   Evapotranspiration  values  for  each cropping season  were developed
including  both periods  when bare soil and/or crops were present.  The results
obtained  for cotton,  grain  sorghum,  and bermuda grass  systems are given, in
Table 3.   For months when  bare  soils and  crops  were  present,  a proportion of
the ET for each condition was computed and summed to obtain the kc value.
                                  TABLE 3

                      MONTHLY ET  AND ET     VALUES FOR
                               p       crop
                        CONDITIONS  AT  LUBBOCK, TEXAS
                                                  ET
                                                    crop
Month
January
February
March
April
May
June
July
August
September
October
November
December
Total
ETP
(cm)
3.91
6.01
10.01
15.84
20.80
26.31
25.98
24.15
16.77
11.78
6.18
4.12
171.00
Cotton
(cm)
2.97*
3.97*
5.21*
6.50*
13.10**
11.57
24.03
29.00
19.96
11.07
3.46**
2.39*
133.23
Bermuda
(cm)
1.40***
2.16***
6.00
15.84
20.80
26.31
25.98
24.15
16.77
11.78
3.59***
1.50***
156.28
Grain
Sorghum
(cm)
2.97**
3.97**
5.21**
6.50**
10.92
17.10
28.32
25.12
10.90
6.83**
2.97**
2.39**
123.20
  *bare soil
 **partially bare  soil  and part cover
***dormant vegetation
                                    23

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Hydraulic Loading  Calculations—
     The hydraulic loading  rate  for  each  test  plot was determined using both
water and nitrogen balances as  design  criteria  (18).  These two calculations
and  the crop coefficients used to  adjust evapotranspiration values  are
described in the following  sections.  .

     Mater balance criteria—Initially, permeability  data published  in  the
Soil  Conservation Service (SCS) Soil  Survey for  Lubbock County, Texas (3)
were utilized as the  basis  for des-ign.   These data had  been obtained from
representative profiles  of  the  soil  series  and  served as  an estimate of soil
water flow conditions at the site.  The results obtained with these data gave
conservative values in  that the  capacity of the soil  profile to  transmit
water  (LWp  in cm  per month) was used as the basis  for the hydraulic loading
rates.  In light of these conservative figures  a series of infiltration tests
was made at each site in July 1982  and  used as the  basis  for-determining
percolation rates.  The split-ring infiltrometer tests yielded  the following
steady state infiltration rates:

           Friona  Ap  series - 46 mm/hr,
           Friona  B22t - 179 mm/hr,
           Amarillo At - 62 mm/hr, and
           Amarillo B22t - 84 mm/hr.

Using the lower values  of  these  data  as  the limiting  condition  for percolate
determination,  new hydraulic loading rates were computed.

     The monthly  hydraulic loading rate (LWp) in cm  of water,  assuming that
the surface runoff of precipitation is zero, can be  defined as:

                        LW  = ET  - P  + P                               (6)
                         p     c    r    w                              v  '
           where ET  = monthly rate of evapotranspiration  of crop in cm,

                P = monthly precipitation (5-yr return period) in cm,  and

                P = monthly probable soil percolation rate in  cm (18).
                  W
The loading rates  obtained for the three cropping systems are  presented  in
Appendix  B.   The  monthly  values of Pw are based on  the  number of operating
days at each site  each week (2.5 days) imposed  by the  irrigation priorities
adopted for the  project.

     Nitrogen  balance criteria—The nitrogen  balances were based on a total
Kjeldahl nitrogen  content of 27 mg/1  N measured in the wastewater collected
at  the Gray site and on 24 mg/1  N wastewater produced  at the Lubbock
wastewater treatment  plant in July  1982.   The configuration  of treatment
processes  used at the  Lubbock treatment plant produced different effluent
streams which caused  the variations in nitrogen content.

     The seasonal  nitrogen needs of the crop were taken  from  the EPA design
manual (18).   The  monthly  nitrogen use values  were calculated by multiplying
the seasonal  nitrogen need by the ratio obtained when  each monthly value  of

                                    24

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evapotranspi ration  for the crop was subtracted from the  precipitation (Pr-ET)
value  for the crop and  the result was divided by the  (Pr-ET) value for the
growing season.

     The monthly  hydraulic load LW/..N in cm of water was computed  by  use of'
the following equation:

          .            _  C0  (*-*W + U 00)
           where  C   =  nitrogen content in mg/1  in percolating water
                 p    (10 mg/1 under EPA guidelines),

                 Pr-ET    = net evapotranspi ration in  cm,
                      crop •
                 U   =  nitrogen uptake by crop  in kg/ha  during the month,

                 f   =  fraction of applied nitrogen removed  by denitrification
                      and volatilization (0.2  used for  determinations), and

                 C.,  =  nitrogen concentration in mg/1  in applied wastewater.

     The values  obtained for  LW(^)  at both  sites are given  in Appendix B.
The hydraulic loading  rates computed  for each  crop  at both  sites  are
presented  in column  5  of these tables.  The  design loading rate (LWg) in cm
of water applied  per month presented  in column  6  of Tables C-l to  C-3 for
each crop  will be  limited  by the nitrogen content of the wastewater  rather
than by soil  permeability.

Irrigation  System

     During the planning phase it was assumed  that a permanent-set  spr'inkler
irrigation system  would be employed on each  plot.  Economic constraints did
not allow utilization  of this system.

     A traveling gun  system*  was  subsequently selected which  utilized
pressurized  treated  wastewater from a permanent pump station on  each site.
Buried pipe was laid from the pump  station  to  risers.   The unit was  equipped
with a  sprinkler nozzle which sprayed in a circular segment over  the area
where the gun had previously  traveled.   The device was capable of  delivering
800 liters  (210 gallons)  per  minute at  552  kN/ma (80 psi)  over a half  circle
with a diameter of 97.5 m under no-wind conditions.  The travel rate of the
unit could  be altered  through a three-speed  gear box and by changing  sizes of
an internal vane  device which affected the initial travel speed controlled by
the gear box.

     The amounts of water applied in each  pass could  also be varied through
*Green Field Traveler, model LD6330.  Manufactured by Boss  Irrigation Equip-
 ment Company,  Lubbock, Texas.

                                    25

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gear box adjustments.   The  speed of movement desired was  from  0.15" to 0.45 m
(0.5 to 1.5 ft) per minute,  which was sufficient to give an  application
volume in each irrigation event of from 4.0 to 6.4 cm over the test areas at
a flow  rate  of 800 liters/minute through the  gun.  The rate of water
application over  a  half circle  with  a  diameter of 97.5  m was .0.213
mm/m"/minute.  The rates of infiltration for  the  two soils  in  the  study were
high  (1.5  to 5.1  cm/hr for  the  Friona soil, and 5.1 to 15.2 cm/hr for the
Amarillo soil) (3) and thus no problem  from surface runoff was  anticipated
prior to the  operational phase.

Irrigation  Schedule—
     The weekly irrigation sequence  for each plot is given in Table 4.  The
irrigation  unit would be at each site  for a 2.5-day period each week.   The
bermuda  grass plots were  irrigated  at both sites on Wednesdays.  In this
manner,  it  was possible  to  irrigate the bermuda .plots at each site  three
times and the other two plots twice during the 2.5-day irrigation interval.

     Also presented are the approximate number of hours  that  were projected
for irrigating the plots at the  time the irrigation system was  designed end
ordered.   The variations  in time were caused by differences  in travel path
lengths and the speed of the gun.   The  hydraulic loading rates  used  for the
irrigation system design were  based  on the rates of soil  percolate movement
in the profile.  The maximum amount of  wastewater to be applied  under the
original design  was 32 cm/month.  The alterations in project loading rates
brought about by field  infiltration tests  resulted  in  an  undersized unit for
project needs.

Measurement of Irrigation Water—
     Because  of the variable area coverage of the irrigation water applied
over the plot due to wind,  a "catch-can" measurement system was developed.
Four plastic  cylinders,  10  cm in diameter  and  15  cm in height,  with weighted
bases, were placed in a diamond  pattern  in which two cans were  in  line  with
the manhole  cover and  parallel  to the  line of  travel  of the  gun.   The
distance between adjacent cans  was from 10 to 15  meters.  The volumes of
water caught in  these  four  cans  were  measured with a graduated cylinder as
soon as the irrigation gun plume had moved past the test area adjacent to the
manhole.

Irrigation Gun Pathways—
     The location of the test sites with respect  to state highways,  county
roads,  and activities on  adjacent parcels restricted  the number of paths
across  each  plot  to one.  Spray  drift caused  by wind  was  the primary
constraint.   The paths  of the gun at each site are given  in Figures 8 and 9.
At the Hancock site,  the bermuda grass plot contained the four  control-tube
lysimeter units in addition  to the  two pairs of 122 cm and  183  cm units.   The
group of eight tube lysimeters at this location was placed in an  excavation
that had been dug in the quadrant southwest from the manhole;  the  traveling
gun crossed over this  installation  on a path  which  had been  selected so that
it was normally just upwind of  the lysimeter battery installation  in the
direction of the  prevailing SW winds.  Though this was to have  insured that
the plot area overlying the  test units got a uniform coverage  of water  in a
majority of irrigation events, it actually influenced the  amount  of percolate

                                   26

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                                             TABLE  4

                                    WEEKLY IRRIGATION SCHEDULE

Irrigation sequence and approximate time in hours
Day
Monday
rv> Tuesday
Wednesday
Thursday
Friday
Site
Hancock
Hancock
Hancock-Gray
Gray
Gray
First
Bermuda (3.7h)a
Bermuda (3.7h)
Bermuda (3.7h)
Bermuda (2.5h)
Bermuda (2.5h)
Second
Cotton (2.2h)b
Cotton (2.2h)
Bermuda (2.5h)
Grain Sorghum (2.5h)
Grain Sorghum (2.5h)
Third
Grain Sorghum (1.4h)
Grain Sorghum (1.4h)
	
Cotton (2.3h)
Cotton (2.3h)
.Speed of 0.3 m/minute
 Speed of 0.45 m/minute

-------
                       Direction | ;
                       of Travel
       Spray Boundary

       Site Perimeter (Fence)
Figure  8.   Irrigation Coverage of  Test Plot  at
            the Gray Site
                           28

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    Qweather Station    _^— Pump

             ©
       Travelling
 \      Gun Track

           ~T
0   15m   30m
     Direction
     of Travel
                            Hydrant
• Direction
: of Travel


I©
                        Test
                        Area
                                                       ....4
•Site Perimeter'
    (Pence)

•Spray Boundary
 Figure  9.  Irrigation Coverage  of Test Plot  at
             the Hancock Site
                           29

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 captured  by  some  of the tube lysimeters on this  plot.   Moreover, the reduced
 water coverage on a plot probably  increased the oasis  effect experienced  by
•the vegetation  grown over the  lysimeters during  the hot,  dry and  windy
 weather  that  prevailed over the  region during much  of the two  growing
 seasons.

 Control Lysimeters—
      Two  pairs of tube  lysimeters collecting soil  percolate at the 1.2 and
 1.8m depths  on the bermuda plot  at the Hancock  site  served as the  control
 system  for the project.  A  metal  structure with a removable  roof was
 installed over these lysimeters.  The sides of the  structure were forced into
 the ground to prevent surface runoff from entering the  enclosed area.   The
 roof was  placed on the structure during wastewater  irrigation periods but was
 removed  during the interim periods to expose the bermuda grass  in the
 structure to sunlight and precipitation.

      Initially,  each irrigation  event on the  control units consisted  of
 flooding  the surface of the enclosed  area with 15 cm  of Lubbock's tap water.
 In the 1983  crop season,  a configuration of plastic pi'pe was used to sprinkle
 the water uniformly over the surface area.

      The  water amounts applied to  the control  plots were to be the  same  as
 the  design  amounts.of  treated  wastewater applied  by irrigation.
 Approximately 15 cm of water was applied "weekly to the plots from June  1982
 through the  second week of November 1982.   Eighteen irrigations were applied
 to the control plots in the interval from March 26, 1983 to August 18, 1983.

 Crops  and Cultural Practices

      The  agricultural  crops utilized in the test plots  were bermuda  grass,
 cotton,   grain sorghum,  and wheat.   The same crops  were grown each season.
 The grass plots were sown with the NK37 strain of bermuda grass.   The winter
 wheat used was  TAM105.   In 1982, Richardson Y-303A®  was the grain sorghum
 variety used, while GSA 1310A was sown  in 1983.  The cotton varieties planted
 were Paymaster 303® and Delta Pine  Rio 875®.   The latter variety was a short-
 season type used  during the 1982 crop season for  replanting after  hail
 damage.

 Project Cultural  Activities—
      Upon completion of the manhole facility,  the plot  areas were filled and
 graded in September and October  1981.   Areas encompassing the manhole and  in
 the vicinity of the aluminum access tubes  for  the neutron probe measurements
 were tilled with  a garden-type self-propelled rptotiller and by hand  tools.
 Wheat was  sown  on all  test  plots.   Calibration of all  the percolate
 collection systems under the same crop and water  management was anticipated.
 With no   irrigation water available  at the site and  the low rainfall that
 occurred  during the fall  of 1981  (3.2  cm  at the  Hancock site from 20 October
 through 31 December,  1981, and 3.5 cm  at the Gray site  for the same period),
 a  poor stand of wheat  resulted.  No attempt was made to harvest the wheat
 prior to plot preparation in March  and April  1982.   The plots were cross-
 disked and harrowed prior  to planting.


                                    30

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     A flat  field surface was  provided for planting.   No herbicides  were
applied on  either  the cotton or grain sorghum  plots since the  use of
herbicides might affect the organic  content of the percolate.

     Wet conditions caused delays in planting and seedling emergence  during
the last two weeks of May.  Establishment of the crops was  hampered by cold
wet soil conditions and hail damage.  The final planting of cotton took place
during the first week of July,  1982.

     The grain sorghum plots were disked and  wheat was  sown  in mid-November.
The unseasonable cold weather which began  the  last week of November 1982 and
persisted through February 1983 reduced the stand  and growth.  The wheat was
disked during land preparation  in March  1983.

     Deep chiseling  of  the four crop  plots  was performed  in  March 1983.'
Because of the weed control  problems experienced during the 1982  season,
herbicide use was  planned  for  the 1983 season.   Treflan® was applied and
incorporated  into the soil on the cotton plots  at  each  site.   The plots were
then  disked and  listed  on  the  contour  in May,  1983.   Milogard®was
incorporated  in the grain sorghum plots  in mid-May.

     Planting of the grain sorghum and  cotton  plots  was completed May  1  at
the Hancock  site and May 24 at  the Gray  site.   A post-emergence herbicide,  2-
4D, was used on  the grain  sorghum plots in June.   The interrow areas were
plowed twice  after seedling emergence.

Weather Monitoring Activities

     Measurements of precipitation and meteorological data at  each site  were
needed  to interpret the results of percolate collection  activities.  The
location of  the instrumentation group in the weather  station  constructed at
each test site is shown  in  Figures  1 and 2.   The parameters  measured at each
site,  type  instruments used, and  frequency of  the  measurements are listed in
Table 5.

Water, Soils  and Crop Analysis

Water Analysis—
     The amounts and quality of the  water applied to  the soil  surface and the
amounts and quality of the  water collected  as percolate by the  vacuum
extraction lysimeters were the  prime interests of the data collection effort.

     Quantity determinations—The input water to the  plot areas consisted of
precipitation and  irrigation with treated wastewater. The precipitation
amounts for  each  test site were measured  with  both  recording  and  non-
recording  rain  gages  located in the weather  station  at each  site.
Precipitation was assumed to have been applied  uniformly over the  2.5 ha
site.   The  amount  of treated  wastewater applied during the  irrigation event
was determined by the catch-can procedure described previously.

     During  the operational  phase of the project, daily  inspections were made
of the lysimeters attached  to  the manhole vacuum systems.   The percolate

                                    31

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                                                    TABLE 5

                                   MEASUREMENT FREQUENCY OF WEATHER PARAMETERS
             Parameters
                                       Type Equipment
                                         Measurement Frequency
ro
Barometric pressure

Pan evaporation

Pan maximum water temperature

Pan minimum water temperature

Precipitation


Radiation - global

Radiation - net

Relative humidity

Temperature

Temperature - wet bulb

Temperature - maximum

Temperature - minimum

Wind speed at 2 meters


Wind speed at 0.6 meters
Microbarograph

Standard evaporation pan

Maximum thermometer

Minimum thermometer

Standard weighing/recording
   rain gages

Pyranograph

Net-radiometer

Hygrothermograph

Hygrothermpgraph

Sling psychrometer

Maximum thermometer

Minimum thermometer

Totalizing anemometer
   with event recorder

Totalizing anemometer
Continuous chart

Daily

Daily

Daily

Daily and continuous chart


Continuous chart

Continuous chart

Continuous chart

Continuous chart

Daily

Daily

Daily


Daily

Daily

-------
collected  in  the 20-liter  glass  bottle which  functioned as the  specific
percolate storage  unit  for  the lysimeter was  measured in a graduated
cylinder.

     Sample collection—Grab samples were taken using all  or a portion of the
daily volume  collected from a lysimeter.  These  were  collected when  a
lysimeter first began percolate  production,  resumed percolate collection
after several  days with no percolate collection,  and during designated sample
collection events.

     Weekly composite samples were  prepared by taking a  portion of each daily
collection volume from the lysimeter.  Composite samples were.also taken with
and without an acid preservative.   The composited samples  were stored in 4°C-
refrigerators  at each site until the end. of the sampling interval.

     Samples of  irrigation water were obtained from the plastic containers
used for determining applied water  volumes.  The collected water from the
four containers" used in the volume  determination was  composited as  an
irrigation water sample for each event on the plot.   The sample was collected.
as soon  as  the plume  from the traveling gun had  cleared the container layout
on the plot.

     Quality  determination—Percolate and irrigation water samples  were
analyzed for  the  parameters presented in Table 6.  The  procedures used are
presented in  Volume I of  Lubbock Land  Treatment System Research _and
Demonstration  Project.  The original  sampling  schedule is listed in Table 7.
The parameters that were analyzed  in  group classification A in Table 7,  were
accorded a priority listing based  primarily  on  the  limited sample volume
collected.  In April, 1983 a sampling schedule was developed to obtain  more
quality  data  from the collected percolate.   The  collection schedule given in
Table 8  consisted of weekly periods in which' composite or  grab samples  were
taken from the lysimeter percolate.  The weekly  composite samples from units
at both  sites  were taken on an as-collected basis or acid-fixed.   Based upon
the  amount  of  sample present,  the analyses to be  run on each  type of
composite sample were prioritized  as  follows.   For the  samples not  acid-
fixed,  the analyses were:   1)  pH; 2) chemical oxygen demand (COD); 3) total
dissolved solids (TDS); 4) sulfate  (S04);  and  5) alkalinity (alk).   For the
acid-fixed samples they were:  1) nitrite plus nitrate (N02+ N03);  2) ammonia
(MHO;  3) total  Kjeldahl  nitrogen (TKI\i); 4) COD;  5) Minerals [i.e., sodium
(Ma), potassium  (K),  calcium (Ca),  and magnesium (Mg)]:  6) chloride (Cl); and
7) total organic carbon (TOC).

     Grab  samples were  taken once a week from each lysimeter  that  had
collected percolate over  the previous 24-hour period  during the designated
periods  shown  in Table 8.   The  sample analysis priorities to be  followed
under the  grab sample collection schedule  were:   1)  conductivity;  2) N03; 3)
orthophosphate; 4) bromide;  5) total phosphorous; and 6) organic phosphorous.

     In  an effort to determine whether solute changes  were occurring  on  a
daily basis,  two  periods  in which daily grab samples were taken from each
contributing lysimeter  unit from  Monday to  Friday  were scheduled.
Applications of 2 kilograms  of sodium bromide were made  over the soil surface
                                  33

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                                                          TABLE 6
                                                       WATER ANALYSES
CO
Alkalinity (Alk) mg/1 of CaCO
Total Organic Carbon (TOG) mg/1
Conductivity mhos
Total Dissolved Solids (TDS) mg/1
PH
Chloride (Cl) mg/Cl/1
Total Kjeldahl Nitrogen (TKN) mg N/l
Nitrite plus Nitrate (NO +NO ) mg N/l
Ammonia (NH ) mg N/l
Total Phospnorus (Total P) mg P/l
Orthophosphate (Qrtho P) mg P/l
Organic Phosphate (Org. P) mg P/l
Biochemical Oxygen Demand (BOD) mg/1
Chemical Oxygen Demand (COD) mg/1
Sulfate (SO ) mg SO /I
Total coliform/100 ml
Fecal Coliform/100 ml
Fecal Strep/100 ml
Salmonella/300 ml
Aluminum (Al) mg/1*
Arsenic (As) mg/1*
Barium (Ba) mg/1*
Boron (B) mg/1*
Calcium (Ca) mg/1*
Cadmium (Cd) mg/1*
Cobalt (Co) mg/1*
Chromium (Cr) mg/1*
Copper (Cu) mg/1*
Iron (Fe) mg/1*
Lead (Pb) mg/1*
Magnesium (Mg) mg/1*
Manganese (Mn) mg/1*
Mercury (Hg) mg/1*
Molybdenum (Mo) mg/1*
Nickle (Ni) mg/1*
Potassium (K) mg/1*
Selenium (Se) mg/1*
Silver (Ag) mg/1*
Sodium (Na) mg/1*
Thallium (Tl) mg/1*
Zinc (Zn) mg/1*
Anthracene/phenathrene PPB
Atrazine PPB
Benzene PPB
Benzeneacetic Acid PPB
4-t-butylphenol PPB
Carbontetrachloride PPB
4-chloroaniline PPB
Chlorobenzene PPB
Chloroform PPB
2-chlorophenol PPB
1-chlorotetradecane PPB
Dibutylphathalate PPB
2,3-dichloroaniline PPB
3,4-dichloroaniline PPB**
Dichlorobenzene PPB M,P,O
DichloroHiethane PPB
2,4-dichlorophenol PPB
Diethylphthalate PPB
Diisooctylplithalate PPB
Dioctylphthalate PPB
Dodecanoic acid PPB
Etliyl benzene PPB
Heptadecane PPB
Hexadecane PPB
Hexadecanoic acid PPB
Methylheptadecanoate PPB
Methylhexadecanoate PPB
1-methylnaphthalene PPB
2-methylphenol PPB
4-methylnaphtlialene PPB
Naphthalene PPB
4-nonylphenol PPB
Octadecane PPB
Phenol PPB
Propazine PPB
Ot-terpineol PPB
Tetrachloroethylene PPB
Toluene PPB
Trichloroethane PPB
Trichloroethylne PPB
         *Total and Available
        **PPB = Parts Per Billion

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                                   TABLE 7



                       SAMPLING SCHEDULE FOR PERCOLATE

Parameter
Alkalinity
COD
TDS
Conductivity
.pH
Total Kjeldahl Nitrogen
NH3
N02+N03
Total Phosphorus
Organic P
Orthophosphate
TOC
Ca
ci.
K
Mg
Na
S04
Heavy Metals
Ag, As, Ba, DC, Cr, Cu,
Pb, Se, Zn, Co, Al, Mn,
Organics
Fecal Col i form
Group Classification*
A
A
A
A
A
A
A
A
A
A
A
A
B
A
A
B
A
B
C
Fe, Hg, Ni
Ti, Mo, B
D
C
*Key:  A - weekly; B - Monthly; C - Quarterly; D - Yearly
                                    35

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co
cr>
                                                   TABLE 8



                                SAMPLING SCHEDULE FOR MAY 1983 TO AUGUST  1983

Percolate
Five Day Daily
Composite Samples Grab Samples Discrete Samples
Month Hancock Gray Hancock Gray Hancock Gray
May Week 1 Meek 1
Week 2 Meek 2
Week 3* Week 3*
Week 4 Week 4
June Week 1 Week 1
Week 2 Week 2 Week 2
Week 3 Week 3
Week 4* Week 4*
July Week 1 Week 1
Week 2 Week 2
Week 3
Week 5 Week 5
August Week 1 Week 1
Week 2* Week 2*
Week 3 Week 3
Week 4 Week 4
Water Quality
Five Day Daily
Discrete Samples
Hancock Gray
Week 4 Week 4
Week 4 Week 4

Week 1 Week 1
   *Acid fixed

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overlying the lysimeters the week prior to  the  first 5-day sampling period  at
each  test area in hopes  of tracing the movement of percolate water through
the profile.

     Also, irrigation waters applied to the test plots were  to be analyzed
for 1) nutrients  (TKN, NO,, NH3, Total  P, PO^  Organic P); 2)  minerals (i.e.,
Na, K, Ca, Mg); 3) COD;  and 4) IDS.   The five-day periods in  which this test
was scheduled- are  listed in the right hand  column of Table 8.

Soil Analysis—
     Core analysis—Soil cores were  taken  within 6.0 m  of the ends of the
lysimeter trays at  various time intervals over  the life of the project.   Each
core was divided  into  30-cm sections,  then those from the same depth at each
test plot were composited to make a sample.-  Soil samples  obtained with the
auger were not subdivided.

     A part  of each  sample was  put into  a glass screw-cap  jar immediately
after segmentation  for priority organic analysis.  The rest of the sample was
put into a sterile  polyethylene bag and sealed.  The samples were then put
into  an  ice  chest and taken to Lubbock Christian College Institute of Water
Research (LCCIWR) for analysis.  The  physical,  chemical,   and bacterial
analyses that were performed on the soil  samples are shown in Table 9.  The
procedures used are presented in Volume I of  Lubbock Land Treatment System
Research and Demonstration Project.  A complete analysis was run during the
first  (March 1981) and  last  (November 1983) sampling periods.   Partial
analyses were run  on  samples taken  in  January  1982 and March  1983 from a few
plots.

     Bromide  analysis—Movement of bromide through the soil profile can
simulate movement  of nitrate (18).  An  application of sodium bromide was made
over different 6 m  by 6 m test areas on each  crop plot each spring during the
test  phase.    Soil cores taken  to  depths of 1.8  m at each  test  area  in
subsequent seasons  were analyzed for bromide so that  the  rate of movement  of
the bromide front  could be determined.

     Soil moisture determinations—Weekly  monitoring of soil  moisture data
began in the  spring of 1982 with a neutron probe,  and continued  through
August  1983 except  for  a few periods  during wet field  or frozen soil
conditions.   Three  access tubes were emplaced on each plot from 5 to 6 m from
the center of the manhole.  The average of  the  three readings  at each depth
on the  plot  was  assumed  to  represent  the  soil  moisture conditions in the
vicinity of the test system.  The readings were made at 15.2  cm intervals
from the surface to depths of 1.5 to 2.1  meters.

Crop Analysis—
     Yield data on each  plot were  calculated from crop samples taken from
three subplot areas that  had been laid  out  parallel with the path of the
traveling-gun irrigation unit and in  line with  the lysimeter battery.   On the
bermuda plots,  the  grass was cut  from  a  grid block with an area of 1  m2 that
had been selected by a random number generation process for each subplot.
The harvested material was put into plastic bags  and taken to LCCIWR for
weight,  moisture content,  and the constituent determinations (Table 10).
                                   37

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                                   TABLE 9
                                SOIL ANALYSES
Alk mg/g CaC03**
TOC mg/g**
Conductivity mhos**
IDS mg/g**
pH**
Cl~ mg/Cl~ Total**
TKN mg/g N Total**
N02/N03 mg/g N**
NH3 mg/g N**
Total P mg/g P**
Ortho P mg/g P**
S0^~ mg/g S**
Organic P**

Organic Matter**

Sulfur mg/g
Specific Gravity
Texture**
Bulk Density**

Color**

Total Coliform/g**
Fecal Coliform/g**
Fecal Strep/g**
Acti nomycetes/g**
Fungi/g**
Al mg/g*
As mg/g*
Ba mg/g*
B  mg/g*
Ca mg/g*
Cd mg/g*
Co mg/g*
Cr mg/g*
Cu mg/g*
Fe mg/g*
Pb mg/g*
Mg mg/g*
Mn mg/g*
Hg mg/g*
Mo mg/g*
Ni mg/g*
K mg/g*
Se mg/g*
Ag mg/g*
Na mg/g*
Tl mg/g*
Zn mg/g*
Acenaphthylene PPB***
Anthracene/
 phenanthrene PPB
Atrazine PPB
Benzene PPB
Benzeneactic acid PPB
4-t-butylphenol PPB
Carbontetrachloride PPB
4-chloroaniline PPB
Chlorobenzene PPB
Chloroform PPB
2-chlorophenol PPB
1-chlorotetradecane PPB
Dibutylphthalate PPB
2,3-dichlorotetradecane PPB
3,4-dichloroaniline PPB
Dichlorobenzene PPB
Dichloromethane PPB
2,4-dichlorophenol PPB
Diethylphthalate PPB
Diisooctylphthalate PPB
Dioctylphthalate PPB
Dodecanoic acid PPB
Ethylbenzene PPB
Heptadecane PPB
Hexadecane PPB
Hexadecanoic acid PPB
Methylheptadecanoate PPB
Methyhexadecanoate PPB
1-methylnapthalene PPB
2-methylphenol PPB
4-methylphenol PPB
Napthalene PPB
4-nonylphenol PPB
Octadecane PPB
Phenol PPB
Propazine PPB
a-terpineol PPB
Tetrachloroethylene PPB
Toluene PPB
Trihloroethane PPB
Trichloroethylene PPB
  *Total and Available
 **Parameters sampled during partial analysis.
***PPB = Parts Per Billion
                                    38

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                 TABLE 10



              CROPS  ANALYSES
pH



TKN mg/g N



NH3 mg/g N



Total P mg/g P



Oil mg/g



Protein mg/g



KCN mg/g



Fatty Acid mg/g



Sulfur mg/g S



Starch mg/g



Niacin mg/g



Fiber mg/g



Biotin mg/g



Total Coliform/g



Fecal Coliform/g



Fecal Strep/g



Al mg/g Total



As mg/g Total



Ba mg/g Total
B mg/g Total



Ca mg/g Total



Cd mg/g Total



Co mg/g Total



Cr mg/g Total



Cu mg/g Total



Fe mg/g Total



Pb mg/g Total



Mg mg/g Total



Mn mg/g Total



Hg mg/g Total



Mo mg/g Total



Ni mg/g Total



Se mg/g Total



Se mg/g Total



Ag mg/g Total



Na mg/g Total



Tl mg/g Total



Zn mg/g Total
                  39

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     Yields of cotton  and  grain sorghum were determined by harvesting the
grain head  and lint over three one-meter lengths of row  from a position on
each  sub-plot  selected by random  number generation.   Weight,  moisture
content,  and the constituents,  shown  in Table 10,  of the bagged samples were
analyzed  by LCCIWR.
                                  40

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                                 SECTION V

                             SYSTEM OPERATIONS
LYSIMETERS
     A number  of problems developed in  the  lysimeter facilities  during the
project.   In  the sections  that follow the  problem areas and the resultant
corrective actions will be discussed.

Flooding of Manholes

     Inundation of  the manholes  with resultant  damage to  the percolate
collection system elicited  the most  concern.  The flooding events were the
result of piping  conditions which  developed when the soil  surface around the
test  facility was flooded from excessive  precipitation.  The tube lysimeters
were minimally affected.

     Piping of water into the cavity of some  of the tray  lysimeters at the
60 cm  level  occurred  on project sites as  a result of  ponding of applied
irrigation water from both sprinkler and flood irrigation events,  and also of
ponding of surface water from excessive precipitation.   Piping  failure in
fill  material  occurred  at one manhole  causing water to enter the  manhole via
the vacuum tube trench  leading from the tube lysimeter battery.  In a few
instances,  piping developed in an area between the pea-gravel layer and the
soil  surrounding the manhole assembly.   In these cases,  water e-ntered the
manhole through tray cavities at the 1.2 and  1.8 meter depths.

     Flooding  from  piping events occurred  at least once  in each of the
manholes  during  the project  period.   Damage to  the systems in the west
manhole  at the Hancock site  and the  north  manhole at the Gray site was not
appreciable since the water depth never rose  to the level where the percolate
collection system was  located.   Flood  damage  at other manholes was extensive
and required  the rebuilding  of the  percolate collection system.   In the
aftermath of these flood events, the vacuum pump unit had  to  be removed and
repaired.   Corrosion of the components  on the  control panels  in the aftermath
of flooding was responsible for at least two  vacuum pump unit failures during
the 1983 crop  season.   Each  flood  event usually deposited  enough  sediment to
cover the bottom of the manhole to a depth of  30 to 60 cm.   The south manhole
at the Hancock site required rebuilding three  times during the active project
phase and each of the other  three units that suffered major flood damage
required two renovations.

     Sump  pumps  with  capacities  of  19 to  30 liters per  minute were not
effective when piping occurred because  of the  large amount of  sediment that

                                   41

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entered the  manhole.  Usually the volume of water entering  the manhole was so
great  that  the sump pump could not have handled the inflow without damage
occurring to the percolate collection  system.

     Problems associated  with flooding were  not  limited to damage  of the
system  components.  There was also  concern that the flows in some instances
were sufficient to  erode soil from the zone of contact between the  soil  in
the top of the tray and the roof of the cavity at the 60 cm level.  The slope
of the  manhole roof was  such  that  only  a 10  or 12 cm opening remained for
the cavity entrance at the 0.6 meter level;  this  prevented inspection of
these  units.  Water from flood events entering the cavities at the 1.2 and
1.8 meter levels caused collapse of  the  wall  sections in some instances.
This could  have  led to a poor interface  connection between  the roof and the
top of the tray.

     In the  aftermath of a flood event, the channels which  had developed from
piping action were  located.  After the soil  had dried,  the channels were dug
out and  the excavated area was backfilled.   In the larger cavities, plastic
bags were filled with soil and tamped  into place.

Vacuum System

     Problems developed  with the original tensiometer design and  in the
associated  operational procedures when the data collection  phase was
initiated.   Some of these problems had been masked  by the dry soil conditions
wh-ich  prevailed  in the  soil  profile during  the  months  of July through
September,  1982.   The moisture levels had  been  generally at soil matrix
potentials greater  than one bar and thus  out of the operational  range of the
tensiometers.  The vacuum levels in  the  lysimeters could  not be adjusted or
evaluated while the tensiometers were  inoperable.  The three primary  problem
areas were:

     (1)  The  use  of deaerated  water  in  the  tensiom&ters, not  having
          prevented gas bubbles from  forming in the horizontal tubing, led to
          inconsistent manometer readings.

     (2)  The use of the flexible thin-wall tubing in the assembly  of the
          tensiometers caused  a varying tubing geometry which led to poor
          reliability in manometer readings.

     (3)  The use  of air, a  compressible fluid,  as the  connecting  fluid
          between  the mercury  in  the  manometers and the water  in the
          tensiometer unit caused a lag in readings.

     The delay in manometer response  was  solved by replacing the air with
water.    The inability to  solve  the first two  problems listed above led to a
decision to  eliminate the original  system  in August 1982.   In September 1982,
commercial tensiometers were  installed as reference units to provide soil
matrix potential data  so  that the vacuum  levels in the tube and tray
lysimeters could be adjusted.   One unit each was installed  at the  60  cm and
120 cm  depths for controlling  the  three tray lysimeters  on the bermuda and
cotton  plots.   A reference tensiometer was placed adjacent  to the 120 cm tube

                                  42

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lysimeters on these  plots.   Tensiometers  180 cm  in  length were not installed
that  fall  because of  the  low matrix  potential readings that were obtained
from the 120 cm tensiometers.  The vacuum levels  in  the  lysimeters at the 180
cm level during the  fall  and winter  season were set  to correspond  to the
readings obtained by the  reference  tensiometers  located at the 120 cm level.
No tensiometers were installed  on the grain  sorghum  plots since winter wheat
was to  be planted.  The vacuum in the lysimeters on the grain sorghum plots
was set to correspond to the readings obtained  in the bermuda grass.

     Shelters,  filled with  insulating material,  had  been constructed  around
the tensiometers.  Despite this,  several  units froze during a cold period
that occurred in the  last week  of November 1982.  Vacuum levels in the other
lysimeters were  thereafter set by  using the  readings obtained  from the
workable reference units at the  same  level.  This approach created a problem
in that some of the reference  tensiometers  had stabilized and portrayed high
matrix potential readings because of the increased  soil water content  from
late  fall  irrigation  events and precipitation.   Units  that were later found
to be inoperable continued  to  record  these  high  readings after soil moisture
content in the  profile  had  decreased.

     The installation pattern used for the commercial-type tensiometers was
not sufficient  for project  control.   Only one tensiometer was installed at
each  depth in  the manhole to control the vacuum in the three trays at that
level  and one tensiometer was installed at the  reference depth in undisturbed
soil  adjacent to each pair of tube lysimeters.   Because of  the  soil
variability that existed around each manhole, this was  probably an inaccurate
way to control  the vacuum in individual trays.

     The vacuum level  in the lysimeters after installation of the commercial
tensiometers was controlled through a system in which a  mercury manometer was
connected to the vacuum line downstream from the  control panel.  The  needle
valve  at the control  panel  was adjusted to give the  desired reading on the
manometer.   The set  point was based on the values obtained from the reference
tensiometer for that depth.

Vacuum System Air Leakage

     The number of connections  between  the wick  assembly in the tray or tube
lysimeter and  the remaining  units  in the percolate  collection system were
minimized to reduce  sites  from  which  leaks could occur.  Each connection was
coated with silicon  sealer  to ensure an airtight  joint.   The connections made
between  the wick assembly in the tube lysimeter and the vacuum tube leading
to the manhole  were  such that the two pieces to be joined were taped together
and then sealed with silicon to ensure that the  joint  was  firmly connected
and would remain sealed after  burial.   In addition,  a  slack length of vacuum
tubing was provided  near each joint so that the soil  stresses on the  buried
lines  would not  pull  the  connection apart.  The vacuum lines from the tube
lysimeter to the  manhole  area were  covered with  soil by hand before the
remaining soil  was placed in the excavation by  mechanical means.

     The primary area where air leakage occurred was  in the wick assemblies
of both the tray and tube lysimeters.   In the first  season  of operation the

                                   43

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reference  tensiometers  initially installed  could  not be used  as control
mechanisms  for the vacuum system.   The  vacuum  level  in each lysimeter unit
was  set  approximately at  the  same point through  adjustment of  the  needle
valve on  the control panel.   Air leakage  into the system in  some manholes was
high and  the number  of  hours of operation of the vacuum pumps  was  excessive.
Adjustment of the vacuum  levels in the  individual manholes was performed to
satisfy the criterion that the number of  hours of operation  generally did not
exceed five to six hours during  a 24-hour period.   In the unit  adjustment
phase it  was noted,  by  the  frequency of  switch operations,  that some
lysimeters  leaked more than others.   These were taken off line.

     The  tube lysimeters  in the north manhole at the Gray site  exhibited
excessive  air leakage when  initially put on  line.   In the  aftermath of a
series of precipitation events in the spring of 1982,  air leakage  decreased
even though no percolate was collected.

     The wetting of the soil profile  during the fall and winter of 1982 led
to decreased air  leakage  in all  the manholes.   Many  tray and tube  lysimeters
began  to collect percolate  and continued to  perform through  the  spring and
early summer of 1983.  As the soil  dried  out due to the deficiency  in amounts
of irrigation water  applied,  the vacuum level  in each  lysimeter unit was
increased  in response to  the  readings  on the reference tensiometers.  This
caused increased vacuum  pump  operation  during the  24-hour period.   Those
units  with noticeable air leakage were again  taken off line.  As  vacuum
requirements increased, the cycle of tray-lysimeter shutdowns followed in
1982 was  again implemented.   The unit with the highest frequency of percolate
collection was left on  line and the other  two trays  at that depth were
disconnected from the vacuum system.  Even so, several  electric  motors  burned
out as a  result of excessive operation  caused  by the vacuum requirement in
the manhole or by a malfunctioning  solenoid valve on  a control  panel.


IRRIGATION

     Problems  experienced  with the irrigation system were  the result  of the
operational characteristics of  the traveling  gun system and  the proposed
irrigation  schedule.

Operational Problems

     The  planned schedule  of irrigation operations  at the  two sites was
quickly found to be too inflexible  with the single irrigation unit  allowed by
budget constraints.  Being  able  to apply the planned  amounts of water  during
the growing season depended upon  the  irrigation unit operating 40 hours per
week.  Any  problems resulting from  irrigation unit maintenance  needs,  stages
of crop  growth,  weather,  water  availability at the site,  field conditions,
labor,  or other project activities would disrupt the irrigation  schedule.
The amounts of water applied to the plot areas were much reduced  during the
two growing seasons, thereby aggravating  problems associated with  percolate
collection  from the  lysimeters.  Insufficient  water application from
irrigation  led to reduced amounts of water that could  drain freely under the
influence of gravity.

                                  44

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Field Percolation Rates—
     Movement  of  the  applied water through the soil  profile was  not as rapid
as had originally been expected.   Hence the soil surface was much wetter than
anticipated  at the  end of  the 24-hour drying period  between irrigation runs.
The  use  of  the 2.5-day weekly  irrigation schedule at each  site caused the
irrigation  gun to retrace  its  path across  the  plots  for two  or  three
consecutive  days  after drying intervals  of  only 15 to  24  hours.   The
consequence  of this was that the soil structure was  destroyed as a result of
the  kneading of  the  soil  by traffic  over the path area and deep ruts
developed.   This treatment  of  the soil  decreased  infiltration rates  and
promoted muddy conditions.  Accordingly, the time for setup of the system
prior to operation  rapidly increased  after irrigation was started each season
due to the depth and expanse of  mud that  had  to  be  traversed.  Due  to  the
operational  sequence followed  in the project, greater stresses  were imposed
by the mud on  both  the vehicle used to transport  and position the irrigation
gun  at  the  plot and on the irrigation gun itself during the  test phase than
would have occurred in normal field operations with a similar  system.

Surface Sealing—
     A factor  which proved influential throughout the project  was the  impact
of the  water  plume from  the irrigation  gun  on the soils at  the test plots.
The height of  the rise of the plume (7  to 10 m above the. ground  surface) and
the subsequent return of large drops  or contiguous volumes of  water to ground
caused severe  erosion.  The erosion effects caused by impact of the plume led
to the destruction  of  soil  aggregates.   -This,  in turn,  resulted in a
reduction of infiltration during the  irrigation events.  The surface  crust
formed  by the disaggregated particles, with possible assistance from the
salts  contained in the irrigation  water during the  drying  cycle,  was
sufficient  to prevent  crop  seeds  from  sprouting  and  to reduce  the
infiltration rates  in subsequent precipitation or irrigation events.

Crop  Damage—
     The impact of  irrigation, water on emerging seedlings caused  a reduction
in the  plant  numbers either through  the washout  of the seedlings or from
breaking the stalks of young plants.  Plant damage was also  noted  at  later
stages  of crop development in  the form  of broken branches, stripped leaves,
removal of seed or  cotton bolls  and broken, bent,  or matted stalks and leaves
in forage crops.

Surface Runoff—
     The wash  or scour caused by the  irrigation  water impact and  flow  was
sufficient to  destroy beds or furrows formed in tillage operations after two
to three irrigation events.  In  the initial year  of  the project  operation, a
flat  field surface  was provided so that the travel of the gun over the plots
would be less  restricted.   The project soils were  assumed to be capable of
infiltrating  water at high  rates,  thus  decreasing the need  for planting on
the bed and  letting the excess water  fill  the adjacent furrows.   The high
infiltration  rates of the  test  plot soils were substantiated by tests made
with  a split ring infiltrometer.

     As the  1982 crop season progressed, the need for a change in the form of

                                  45

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the field surface  became apparent.  Large amounts  of  the applied water became
surface run-off and  collected in the  ruts of the irrigation unit  path  or
flowed to low points on or outside  the test  area.  The amounts of water that
were  collected in  the  catch-cans were  not representative of  the water
infiltrating  into the soils over the  test units  in  view of the  runoff
observed during the  irrigation events.   The  flat field surface and the scour
action of the water  upon impact,  which sealed  the soil surface, aided in the
generation of surface runoff.

Field Activities—
     The accumulations of  runoff in the low areas  increased the difficulty of
performing cultivation and of setting up the  irrigation gun system prior  to
an irrigation event.  In some instances, because of the persistent expanse of
mud  along  the irrigation unit path,  turn rows were  constructed  during
cultivation along  the boundary of the muddy'areas, thus destroying additional
test plot vegetation.

Corrective Measures

     The problem  areas previously outlined  were  addressed during the
operational  phase  of the project  as  discussed  below.   Remedial actions taken
to minimize or eliminate operational problems  experienced in  1982 are
presented in the following discussion.

Plume Impact—
     A plume  dispersion device  was installed on the irrigation gun late in
the 1982 crop season.   This aided  in  the dispersion of  the water  jet  and
helped modify the  rates of erosion from soil  splash and surface scour.

Crop Damage—
     Irrigation events were delayed on  the crop plots  during the 1983 growing
season  until cotton and  grain sorghum seedlings  had  emerged and were in the
early phases of the  crop development stage (crop ground  cover >10%).   This
increased the stand  of plants on the crop  plots but eliminated the amounts  of
wastewater that were scheduled for application  during  that time interval.

Surface Runoff—
     A major concern during  early months  of  the 1982  growing season was that
the amount of applied water could not be correlated with the"amounts of water
infiltrating into  the soil over the test lysimeters because of the observed
runoff  during irrigation.  Water was  held on  the site by constructing dikes
in September 1982  around the test area  containing the  lysimeters.   The  plan
was to dike three  plots of similar size parallel to the path of the traveling
gun.   The center plot area had  15 m sides.   This  length was somewhat greater
than the diameter  of the lysimeter battery (9 m).   The plots adjacent to the
center plot were to  be used for crop yield measurement.

     Crop and  weed  residue on the cotton and  grain  sorghum plots produced a
mixture of organic and inorganic material in the dike.   The resistance  of
this mixture to the scour of the plume was  lower than that which would have
occurred with soil alone.  The dikes on the  crop plots  became ineffective
after only 2 or 3  sequential irrigations in the fall of 1982.

                                   46

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     Construction of the dikes  in the bermuda grass  plots was hindered by wet
soil conditions  and the thick grass sod.  The addition of irrigation water,
however,  caused the sod in the dike material to  begin  new growth.   This
regrowth  provided much more stability to the dikes  in the bermuda grass areas
than was experienced on the  crop plots.  The applied water was effectively
retained  in the diked plots during the fall and winter months.

     In March 1983,  the  dikes around the bermuda  grass plots were
reconstructed prior to new vegetal .growth.   Because of the observed failure
of the  dikes on the crop plots  during the previous  fall,  contour furrows  on
the crop  plots were constructed with a lister after  running guide rows with a
level.   The contour furrows  were eroded by plume  scour but were maintained
over the crop season by cultivation.   Problems  still  resulted with  the
excessive mud in the vicinity of the path of the  traveling gun since in all
plots the path of the gun was generally perpendicular to  the contour  rows.
These wet areas  caused problems in cultivation.  Nonetheless, surface runoff
from the  plots was reduced  by employment of the contour rows.

     The  expanse of  mud created by the  movement of the  gun  in  a path
perpendicular  to the contour rows and the roughness  of the traveling gun path
in the aftermath of furrow construction or reconstruction by cultivation
increased the  time required to  set up the system prior to an irrigation event
above that experienced in the  previous crop season.   Field roughness,
resulting from the crossing of  each furrow and bed,  also added  to  the
stresses  imposed on the irrigation and transport units, causing an increase
in down time  of  both the traveling gun and the transport system during the
1983 crop season.
                                  47

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                                SECTION VI

                           RESULTS AND DISCUSSION
     Results  of  this  study ideally would be presented  in  tabular  form so the
changes in mass  flux  of  the  quality parameters resulting  from input, output,
and storage in the root zones of the test  plots  for specific  time periods
could readily be seen.  Since movements  of  organic and inorganic constituents
of concern in municipal wastewater land application systems are dependent on
the water flux in the soil profile,  the  occurrence, composition,  state, and
rates  of  water  flow in the profile must be  known to determine the  transport
and fate of wastewater constituents.   Failure to  apply the  design  rates of
treated wastewater on the  test plots  caused soil  moisture  levels in the
profile that  were insufficient to generate  percolate continuously  during the
project.   The  inability to intercept  the percolate that was generated with
the  installed  collection devices, and to  measure  evapotranspi ration
accurately over the project period on  the test plots has made it impossible
to calculate accurate and  meaningful   water balances and  have,  thereby,
diminished the utility of the project  results.

     The inability to  account  for the water flux also limits the  interpre-
tations that can  be made about the  fate of the various  constituents of
concern  in municipal wastewater land  application  systems since the  transport
of these materials is dependent on the  water flux.   In addition,  good and
complete  data  regarding solute concentration,  mass, and  location in the
profile were  unavailable, as  was a definite  knowledge of the  interactions
(i.e.,  sorption, precipitation,  dissolution,  etc.) occurring between the soil
matrix  and the  soil  water.   Quantification  of all this information would be
essential  in  order to determine the fate of pollutants in the  soil  matrix,
ground  water,  or  crops, and  in order  to  obtain  a complete understanding of
the many chemical,  physical,  and biological  processes which  comprise the
system.

     The hydrologic  portion of the  study was planned to obtain  information
that could be used to evaluate the masses involved in the following equation:

          (Precipitation + Wastewater Applied  in Irrigation)  =
          (Evapotranspiration + Percolate Flow from the Root Zone
                             + Change in Root Zone Water Storage)        (8)

     Information on the solutes that posed  possible quality impacts  to the
soil,  crops, or the underlying ground  water  was  sought to help evaluate the
terms (in  kg/ha) of the following equation:
                                   48

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          (Mass  applied in Irrigation Water)  = (Mass  removed in Harvested
          Crops  +  Change of Mass in the Internal  Storage  Elements in the Root
          Zone Profile + Mass Transported out of  the  Root Zone in Percolate +
          Mass Transported out of the Root Zone as  Gas)                   (9)

As an example of what was expected in the study,  the  design hydraulic loading
rates from Table C-l and the climatological data recorded  at the  site from
May  1,  1982, to November  17,  1982, were used to  develop a scenario of what
should have happened on the bermuda grass plot at the Hancock site for water,
total nitrogen,  and total phosphorous.  The following data  and assumptions
were used to estimate the results:

     (a)  The bermuda grass that was planted  in May,  1982, was irrigated with
the design requirement for May as shown in Table" C-l  (55  cm).

     (b)  The irrigation water applied to the plot  exhibited a total nitrogen
content  of 37.7 mg/1 and  total phosphorous of  9.06  mg/1  throughout the
irrigation season.  (These  values  represent the  geometric mean of five
analyses  of each constituent obtained from  five samples of irrigation water
collected in catch  cans on the Hancock site in the  summer of 1983.)

     (c)  The amounts of bermuda grass produced and  the  protein content of
the harvested grass are proportional to the amount  of nitrogen applied in the
irrigation water  (16).   [Estimates of the hay  produced  and the protein
content were developed by extension  of log — log diagrams  constructed from
yield  data presented in a Texas Agricultural Extension  Service publication.
(22)]'

     (d)  The nitrogen content of the dried bermuda grass was 16 percent of
the protein content (13).

     (e)   Since applied nitrogen governs crop production to a large extent,
the amount of phosphorous removed by  the  crop was  dependent on the amount of
nitrogen  applied to the grass.   [Removal  rates  were  from 35 to 45 kg-P/ha
over the range of  nitrogen applications from  400  to 675 kg-N/ha (18).]

     (f)  Denitrification and volatilization caused a 25 percent loss  in the
amount of applied  nitrogen (18).

     (g)   The nitrogen  not utilized in  the  growth of  the bermuda grass or
volatilized remained in the soil water.

     (h)  The phosphorous in the applied water was  removed  in the  root zone
by specific adsorption and precipitation (10),  while no nitrogen was stored
in the root zone.

     (i)  Evapotranspi ration losses from the  bermuda  grass  were similar to
those calculated by the following equation (5):

          ET    -  KK                                               (10)
            crop
                                    49

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          where ET     = monthly crop evapotranspiration in cm

                    K  = pan  coefficient

                    K  = crop coefficient
                     c
                 ET    = monthly Class A pan evaporation in cm
                   pan

The values obtained for the hydro!ogic factors during the May to November
time interval  were as follows:
          [60.5 cm (precipitation) + 305 cm (applied wastewater)] =
          [86.18 cm (evapotranspiration) + X cm (percolate flow from the root
          zone)].

The depth of percolate  flowing to the ground water was calculated from  this
analysis to be 279.32 cm.   The. volume of percolate per hectare flowing from
the root zone  would thus have been 28,000 m3.

     Using the total  nitrogen and  total  phosphorous concentration of the
wastewater and the design irrigation  rates,  the amounts  of the two nutrients
were computed  employing the assumptions previously made.   These values  were
inserted into  the equation for solutes as follows:

Calculations for total  nitrogen,

          [780 kg N/ha  (applied in irrigation water)] = [(0.25 x 780) kg N/ha
          (volatile losses) + 0 kg N/ha (storage in the root zone) + (0.122  x
          0.16 x 21,000) kg  N/ha (removed  in the harvested crop) + Y kg N/ha
          (transported  out of the root zone in the percolate)].

The value obtained for  Y was  173 kg N/ha.   Using  the values  calculated for
nitrogen and  the  percolate,  the concentrations of nitrogen in the percolate
flowing from the root zone would have been 6.18 mg N/l.  This value meets the
design criterion for percolate flowing into underlying ground waters (18).

Calculations for total  phosphorous,

          [276 kg P/ha  (applied in irrigation water)] = [Z  kg  P/ha  (storage
          in the root zone) + 48 kg P/ha (removed in the harvested crop) +
          0 kg P/ha (transported out of the root zone in the percolate)].

The value of Z was 228  kg P/ha.   This amount should have been accumulated in
the soil during the 1982 growing season.

     In contrast to what should have happened, data that were  obtained  from
the project were  used to  compute corresponding values in equations (8) and
(9).   The rainfall and  the evapotranspiration values used were the same  as in
the previous evaluation. The actual  irrigation amount,  99.17  cm (Table 12),
that was applied  was  only  32.5 percent of the design amount.  The average
depth  of percolate  intercepted by  the  surface area  of the five   tray
lysimeters operative  during the period was 0.4 cm.  Utilizing the measured
hydrologic data,  the following results were obtained:

                                    50

-------
          [60.5 cm (precipitation) + 99.17 cm (applied wastewater)]  =
          86.18 cm (evapotranspiration) + 0.4 cm  (percolate flow from the
          root zone) + Y cm (unexplained losses)].

The unexplained losses in the  183 cm depth of soil  that was monitored on this
plot during  the 1982 crop season amounted to a depth of approximately 73 cm
of water.   The  data collection techniques used were incapable of detecting
this loss.

     The  total  nitrogen and  total  phosphorous values  used  in the solute
equation  were developed from crop, soil, and percolate samples.  The nitrogen
and phosphorous  associated with crop production were developed from  grass
production figures on the  test plot (Table 19) multiplied  by the average
total, nitrogen (30.4 mg N/g) and  the average total phosphorous (3.04 mg P/g)
obtained  from analysis of grass samples harvested  from the  plot during the
1982 season.  Values of organic nitrogen-N, NH3-N, N02+ N03-N,  and  total
phosphorous-P obtained from soil samples taken on  the plot  (March 1981 and
February  1983 for NH3 and N02+N03,  and March 1981 and November 1983 for
organic nitrogen  and -total phosphorous) were used  to determine the  change in
the mass  of nitrogen and  phosphorous in the  183-cm profile depth.   The
estimated mass  of soil (25,560 metric tons) was derived from soil  bulk
density  values  obtained from samples taken on  the plot.  Average percolate
concentrations for total kjeldahl nitrogen, NO,+ N03-N, and total phosphorous
for the tray lysimeters on the plot  (Table D-1) were used  to  determine the
amounts  of  the  two nutrients transported in the percolate.  Use of  these
values  in the solute equation  gave the  following  results:

Calculations for  nitrogen,

          [780  kg N/ha (applied in irrigation water)] =  [3,440  kg  N/ha
          (decrease in storage) +  72.4 kg N/ha  (removed  in the harvested
          crop)  - 4.0  kg  N/ha  (transported  out of the root zone in the
          percolate) + Y kg N/ha (unexplained losses)].

Calculations for  phosphorous,

          [276 kg  P/ha  (applied  in irrigation water)]  = [424 kg P/ha
          (increase in storage) +7.1 kg P/ha (removed in the harvested  crop)
          +  0.002
          kg P/ha (transported out of the root zone in the percolate) +
          Z  kg P/ha (unexplained gains)].

The value of the  unexplained  losses in nitrogen, Y, was  calculated to be
2,584  kg N/ha,  whereas  the unexplained gains, Z, in  phosphorous were
approximately 141 kg P/ha.   Even if  100 percent of the applied nitrogen was
assumed to be  converted to gas  through volatilization  of ammonia and
denitrification,   an unexplained loss of 1800 kg  N/ha occurred that was not
accounted for in  the percolate or in crop removal.  The solution obtained for
nitrogen  was in  contradiction  with  the expected  result.   The result obtained
for phosphorous, a material easily removed   in  the soil  matrix,  was
satisfactory  and would have been  even better had the geometric mean of the
wastewater total  phosphorous  content been used.  However,  there are some

                                   51

-------
questions associated with the data obtained for total phosphorous  in the soil
profiles during the March 1983 and the  November 1983 sampling  events (Table
26).  Average  profile values  for March  1983  showed an increase since the
initial  sampling period  in  March 1981  in 5 of  the 6 plots.   The results
obtained in November 1983 showed that,  in 4 of  the 6 plots,  the  average
values  of total phosphorous in the profile had decreased below the values
obtained in March  1981.   Results obtained with mass balance calculations were
changed from unexplained losses to unexplained gains when using  the different
sets of data as  the basis for calculations.

     Conducted in  a manner similar to that used for N and  P, a  mass  balance
for chloride,  calculated for the same time period,  showed that 3,300 kg Cl/ha
was  applied and  that  the soil  content of chloride  in the  183 cm  depth
increased by 1,330 kg  Cl/ha.  Crop use and  percolate flow accounted for
losses  of 1.5 kg Cl/ha and 32.3 kg Cl/ha, respectively. . Unexplained losses
of chloride in the soil  profile on this plot amounted to 1,928 kg  Cl/ha.

     The magnitude  of  the unexplained  losses in  the soluble  components
transported out of the profile during the 1982 crop season on  this one plot
illustrates the  difficulty associated with attempting to utilize mass balance
determinations to  explain the phenomena occurring on and below the test plots
in this study.

     Moreover, irrigation loadings during the primary seasonal growth periods
on the other plots were smaller percentages of the design  load  (Tables  C-l,
C-2, C-3, 11,  12,  13, and 14).  Crop yields on the test plots were lower than
those  attained  on similar  area sites  irrigated with ground water.   The
erratic yield  and infrequent occurrence of  percolate events led  to  even
greater  infrequencies in percolate quality sampling events  and analyses
(Table D-l).   Also, the study procedures  used  were incapable of  monitoring
the water and  solute flux in the internal storage elements  of the  soil matrix
in  an  adequate  and timely  manner.  These irregularities in the  project
operation,  coupled with inadequate data collection, would require  unjustified
manipulation of  the available information in  order to obtain  mass  balance
determinations.  Therefore,  the use of  material balances in the  explanation
of the project results was not attempted.  In the following sections,  the
results  that  were obtained  during the project  period  are presented and
discussed in the context of the observed  events.


PERCOLATE COLLECTION ACTIVITIES

Hydraulic Loadings

     Lysimeter operations  began at both sites  in May 1982 and continued
through September  1983.   The  precipitation  and irrigation  records  at the two
sites for the  two  growing seasons are shown in Tables 11 and 12 for the 1982
season and Tables  13 and  14  for the 1983  season.  Annual  estimated
evapotranspiration amounts, shown as ET0  in the tables,  were calculated using
actual  pan evaporation data obtained  at the site and a pan  coefficient
multiplier,  Kp,  that was selected using monthly geometric means  of wind speed
and relative  humidity as criteria (5).  Also shown are estimates of ETcr0p

                                    52

-------
                                                 TABLE 11

                               HYDROLOGIC FACTORS AT THE GRAY SITE FOR 1982



Month Precipitation
(cm)
January
February
March
April
cn May
Co
June
July
August
September
October
November
December
TOTAL
0.41
0.48
1.42
4.04
19.30
15.52
4.75
1.80
4.42
1.50
3.53
3.30
60.47
Input
Applied Uastewater
Bermuda Cotton Grain Sorghum ET a
(cm) (cm) (wheat)(cm) (cm)
3.06C
8.04C
14.21
15.77
10.88
12.26
21.35 5.35 14.16 18.11
20.29 10.05 11.80 14.38
18.93 14.34 14.57 13.33
31.55 7.78 11.26
4.44 6.43
3.55 4.15C
92.12 37.52 48.52 131.88


Bermuda
(cm)



8.70
11.03
16.30
12.94
12.00
10.13
3.21

74.31
Output
ET b
crop
Cotton Grain Sorghum
(cm) (cm)




5.44 5.44
7.23 9.26
17.93 19.74
17.26 14.60
15.86 7.83
10.75
4.63

79.10 56.87
aSummation of daily data measured during month that was multiplied by pan coefficient K  ( 5 ).   In each
 month there were some daily data missing because of ice, rain, or the water level  in tRe pan being too
.low for accurate measurements.

   crop = ^C^Q) wnere KC is a crop coefficient ( 5 ).

clce in the pan for several days.

-------
                                                 TABLE 12

                             HYDROLOGIC FACTORS AT THE HANCOCK SITE FOR 1982



Month Precipitation
(cm)
January
February
March
April
May
June
July
August
September
October
November
December
TOTAL
0.78
0.58
3.20
2.16
18.64
19.74
11.28
2.72
4.42
0.83
2.95
3.14
70.14
Input
Applied Wastewater
Bermuda Cotton Grain Sorghum ET
3 o
(cm) (cm) (wheat)(cm) (cm)
4.58C
6.33C
•12.46
18.99
14.90
13.31 8.85 1.73 12.62
14.22 12.33 13.11 20.33
14.05 13.00 8.77 19.10
18.84 16.81 13.03 13.20
22.00 6.45 1.50 13.54
16.75 6.68
4.26C
99.17 57.44 38.14 146.99


Bermuda
(era)




11.92
11.36
18.30
17.19
11.88
12.19
3.34

86.18
Output
ET
Cotton
(cm)




7.45
7.45
20.13
22.92
15.71
12.93
4.81

91.40

b
crop
Grain Sorghum
(cm)




7.45
9.53
22.16
19.39
7.76



66.29
 Summation of daily data measured during month that was multiplied by pan coefficient K  ( 5 ).  In each
 month there were some daily data missing because of ice,  rain, or the water level In trie pan being too
,low for accurate measurements.
 *^crop = "c^^o^ wliere *  is a cr°P coefficient ( 5 ).
 Ice in the pan for several days.

-------
Wl
tn
                                                                           TABLE 13

                                            HYDROLOGIC FACTORS AT THE GRAY SITE FOR JANUARY 1  TO SEPTEMBER 30.  1983
Input
Applied Uastewater
Month Precipitation
(cm)
January
February
March
April
May
June
July
August
September
TOTAL
5.00
0.78
0.45
1.58
11.08
5.54
3.38
0.00
0.60
28.41
Bermuda
(cm)


6.39
4.81
5.56
16.74
4.86
4.74
5.99
49.09
Cotton
(era)



4.78


4.87
8.84
2.41
20.90
Grain Sorghum
(wheat)(cm)



3.10


6.57
3.67
5.92
19.26
(cm)
1.48C
5.24
9.46
14.58
18.45
16.07
20.68
9.29d

95.25e
Bermuda
(cm)


7.57
13.12
16.61
14.46
18.61

70.376
Output
ET b
crop
Cotton Grain Sorghum
(cm) (cm)




9.23 9.23
9.48 12.13
20.47 22.60

39.186 43.96e
                           3Summation  of daily data measured  during  month  that  was multiplied  by  pan  coefficient K  (5).   In each
                           month  there were  some daily data  missing because  of ice,  rain, or  the water  level in tne pan being  too
                           .low  for  accurate  measurements.
                           DETcro  = Kc(ETQ).where KC  Is  a  crop  coefficient ( 5).

                           clce  In the pan  for several days.
                            Pan  water  level too  low  for  accurate measurements.
                          eTotals do not represent data from entire growing season.

-------
CT>
                                                                            TABLE  14

                                           HYOROLOGIC FACTORS AT THE HANCOCK  SITE  FOR  JANUARY  1  TO SEPTEMBER 30.  1983
Input
Applied Wastewater
Month Precipitation Bermuda
(cm) (cm)
January
February
March
April
May
June
July
August
September
TOTAL
3.20
0.41
0.76
2.59
6.89
3.20
3.12

0.60
20.77


12.22
9.02
16.29
24.98
19.92
8.44
59.70
150.57
Cotton Grain Sorghum ET a
(cm) (wheatHcm) (cm)



6.63 4.60

4.87
14.65
16.02 14.04
40.60 5.92
82.77 18.64
3.13C
3.84C
• 10.12
12.94
13.65
20.63
23.20
17.40

111.46d
Output

ET b
crop
Bermuda Cotton
(cm) (cm)


8.10
11.65
12.29 6.83
18.57 12.17
20.88 22.97
15.66 20.88

87.15d 62.85d
Grain Sorghum
(cm)




6.83
15.58
25.36
17.66

65.43d
                            aSummat1on  of daily data  measured during  month that was multiplied by pan coefficient K  ( 5 ).   In each
                             month  there  were  some daily data missing because of 1ce,  rain,  or the water level in tRe pan being too
                            . low  for  accurate  measurements.
                             ETcrop " Kc*EV  where Kc 1s a  crop Coeffic1ent ( 5 ).
                            jlce  In the pan for several  days.
                             Totals do  not represent  data from entire growing season.

-------
which were  calculated using  the estimated  ET0 and  a  crop  coefficient
multiplier,  Kp,  selected by using wind  speed,  relative humidity,  and  stage of
crop growth  as  criteria (5).

     The hydraulic  loadings applied to the control plot at the Hancock  site
are not shown  in Table 11 or Table 13.   The  bermuda grass  on  this plot was
irrigated  with potable water from the  Lubbock system over  both growing
seasons in  the  test period.  The hydraulic loading rates (approximately 240
cm in 1982  and 270 cm in  1983)  and  the water  quality differences between the
control  plot  and  the test plots were so different  that no meaningful
relationships  could be developed using  the control plot data.

     The percentages of the design irrigation application rates (Tables C-1
to C-3)  that were  actually  applied in  1982 to the bermuda  grass,  cotton, and
grain  sorghum plots  were 27%,  83.5%,  and  60.7%  at  the Gray site.  The
calculated  values  for  ETcrop for the three  test  crops in  Tables 11 and 12
were lower  than those which were  used  to  estimate the design  hydraulic loads
(Table 3).   Monthly totals of applied  irrigation water and  precipitation
exceeded the calculated values for ETcr0p  over the 1982 growing season  on.the
bermuda grass  plot at the  Gray  site  and for all  months of the  growing  season
except August  at the  Hancock site.  The calculated ETcr0p for  cotton  exceeded
the water inputs in July, August,  October, and November at the  Gray site, and
in August,  October, and November at the Hancock  site.  Hydrologic loadings
exceeded the calculated ETcrop for the  grain sorghum except for the months of
July and August at the Gray site,  and  for the month of August  at the Hancock
site.

     The monthly amounts of irrigation water  applied to the plots during the
1983 growing season,  shown  in Tables 13 and 14, were below design loads.  The
percentages of the design application  rates applied to the plots for the
bermuda grass,  cotton, and  the grain sorghum  at the Hancock site were  44.8%,
17.5%,  and  18.4%,  respectively.   At  the Gray  site, the respective rates  were
15.8%,  46.6%,  and  24.4% of  the design loadings for bermuda grass,  cotton, and
grain sorghum.  The  calculated values  of ETcr0p  for bermuda grass were
greater  than  the  applied  hydraulic loadings except for the  months  of April
and August  at  the  Hancock site and for  the month  of June at the Gray site.
On the  cotton and grain sorghum plots at both sites, the hydraulic  loadings
were greater than  the  calculated values of ETcr0p only in  the  month of May
during  the  period March  through August, 1983,  after which  pan evaporation
data collection was discontinued at both sites.

     Soil moisture conditions during the growing  seasons were much drier  than
the ETcr0p  values that were predicted using pan evaporation data.  Soil
moisture values calculated using  recorded  percolate events from the
lysimeters  gave evidence of dry soil  conditions.  The inability to apply
irrigation  water  at  the design rates  during  the two growing  seasons was the
cause of the low number  of percolate collection events  recorded during those
periods  critical  to  the study.  Problems experienced during  the two growing
seasons accounting for the decreased irrigation amounts are presented in the
following subsections.
                                    57

-------
1982 Season-
     Precipitation recorded at the sites  in the six months prior to  May  1982
were 73.5 percent of the long  term average at  the  Gray  site  and 69.5 at the
Hancock site.   Irrigation water became  available  for use at the Hancock  site
in April  and at the Gray site in May.   No pre-plant irrigations were applied
at either site  because of the timing of the availability of irrigation water
at the sites and the existing  time constraints imposed  by equipment and labor
availability for land preparation  and planting operations of the three crops
at the two sites.

     Storm conditions  in May  and  early June caused delays  in planting,
problems  with seedling emergence,  and  hail damage  to   seedlings.
Additionally,  the  vacuum  units had  to be repaired  and  the percolate
collection systems rebuilt after the manholes  on the cotton and  grain sorghum
plots  at both  sites were flooded  in  the aftermath of  high  intensity
precipitation  events during  this time period.  The grain sorghum plots  were
replanted in late May and the  final  replanting of the cotton  plots with  a
short season variety occurred  in early July.

     After the  delays caused by the  replanting operations  and  the repairs of
the flooded manholes, irrigation applications were started in June at the
Hancock site.  Startup problems  occurred with  the  pump  station.   Construction
debris in  the  pipe  laid to the test site clogged the  pump impellers several
times during the initial pumping  period, causing multi-day  delays.  When
irrigation operations were started at the Gray site in July, the clogging of
the pump  impellers in the booster  pump at the  site caused  further delays in
the  irrigation  schedule at both sites.  Additional problems experienced
during the growing season,  which collectively  aided in  reducing the  amounts
of irrigation water applied to the plots,  were:  (a) postponing  irrigation to
prevent seedling  damage (cotton  plot at  the Gray site),  (b) delaying
irrigation so that the crop plot  soils would dry enough  to  cultivate for
weeds,   (c) maintenance problems with the traveling  gun system,  (d)
maintenance problems with the  vehicles  used to position  the  traveling gun
system,  and (e)  the inability to obtain water at the Hancock site  prior to
midmorning.

1983 Season-
     One  prewatering event was applied to each crop plot in  April 1983.   No
irrigation water was applied to  the crop  plots in May  because  of land
preparation and planting operations.   To prevent damage to seedlings  from the
irrigation gun  plume,  irrigation was delayed   on the crop  plots  until
sufficient growth had been attained.

     When the cotton was  irrigated on  June 21  at the Hancock  site plant
damage occurred.  Irrigation was then delayed  further  on  the crop plots at
both sites.  This  delay in initiating  irrigation caused decreases in  soil
moisture  by the end of June.

     Problems  with  the  traveling  gun  system  developed during  June.
Thereafter maintenance operations associated  with the  muddy field conditions
and the unit braking system, cable, and  cable  guidance  system during  July and
August caused multi-day losses of  irrigation application events.  A  traffic

                                   58

-------
accident on  August 3 disabled, for the remainder  of  the project, the vehicle
used for  positioning the traveling  gun in the field  and  injured one of the
two full-time  employees on the project.   The irrigation gun was subsequently
operated only  eight more days in  August.

     In an effort to  raise  soil moisture levels to a point where percolate
could  be  generated  in the  soil  profile for capture by the extraction
lysimeters,  wastewater effluent was  applied in flood  irrigation events on the
cotton  and bermuda grass plots at the Hancock site  in  September.  Irrigation
efforts continued during September at  the Gray site  using  the traveling gun
unit.

Percolate Quantity

     Only 25  of the  41  lysimeters on the  Gray site contributed percolate
during  .the five months of the 1982 growing season.  At  the Hancock site,  26
of the  46 units  had contributed percolate by  the end  of September.  The
increased amounts of irrigation in August and September and decreased  rates
of evapotranspiration in the latter part of the  growth period led to an
improvement  in soil moisture conditions and an  increase in the number of
percolate collection events during September and October 1982.

     The buildup of  moisture in the soil  profiles of all the  plots as a
result  of fall irrigation, fall  precipitation,  and decreased evaporation
subsequently led to percolate generation in many lysimeter  units that had not
contributed  previously.  By December 31> 1982, 35 of  the 41  units on the Gray
site had  contributed percolate, and at the Hancock,  30  of the 46 units had
contributed.   Percolate collection events continued on a'frequent  basis
through  February for many  of the  contributing lysimeters,  but by  March
decreases were noted.  Percolate  events and the amount  of  percolate collected
per event decreased through May in most lysimeter units.   A low number of
percolate collection events  occurred during the crop growing season on all
plots  as  a  result of low soil  moisture  levels  in  the soil  profiles.
Percolate collection events  were  noted in two more  units on the Gray site
during  1983  so that flows from 37 of the 41 units at  the Gray site occurred.

     As an example of the percolate  amounts and occurrence  experienced during
the study period, Table 15 presents  the depths of percolate in mm intercepted
by the  surface area of the various lysimeters on  the bermuda grass  plot at
the Gray  site.   The low amounts of  precipitation  received during the three
months  prior to May 1, 1983,  (41  percent of average  rainfall) and the 1.29 cm
of rain occurring in May before a storm event of May  30 which produced  9.78
cm of  precipitation had caused a decrease  in the  volumes of percolate
produced in  the  lysimeters on  this plot.   The monthly  percolate interception
in all  but the 183 cm and 244 cm  depth tube lysimeters  had  decreased to below
1  mm depth  by the end of May.   Even though  irrigation on this plot had
started in March, the amounts produced by the  four  longer tube lysimeters
continued to decrease over the next  three months and  had ceased by September.

     Percolate was collected from tray units at all  depths in October 1983
following  flood  irrigation  of  the bermuda grass  plot in September.
Additionally,  two tray units  located at  the  60  cm level on  the bermuda grass

                                   59

-------
                                                     TABLE 15

                              MONTHLY PERCOLATE DATA IN mn FOR THE BERMUDA GRASS PLOT
                               AT THE GRAY SITE FROM OCTOBER 1982 TO SEPTEMBER 1983

Tray Lysimeter Units
61 cm 122 cm
Month 101 102 103 104 105 106
Oct. 1982
Nov.
Dec. 12.4 6.8 0.5
CTl
0 Jan. 1983 21.7 8.1
Feb. 20.2 2.3 2.1 5.6
Mar. 5.6 0.3 0.3
Apr. 0.4 0.6
May 0.7 0.2
June
July
Aug.
Sept.
Tube Lysimeter Units
183 cm 122 cm
107 108 109 111 112
61.9
• 100.2
9.4 6.5 2.6 52.2 40.8
5.6 10.2 3.7 35.1 19.6
5.8 15.4 4.7 46.4 32.1
7.3 6.3 2.0 9.9 10.7
1.9 2.9 0.4 4.0 3.9
0.7 0.8 <0.1 0.4
0.1 0.4 <0.1
<0.1 <0.1
0.3
<0.1
183
113


13.6
22.4
29.1
7.0
5.7
12.2
5.5
3.6
1.4

cm
114


51.9
22.6
39.6
7.9
2.7
10.0
3.8
1.3
0.2

244
115


109.2
43.9
65.4
32.6
16.6
12.2
3.8
4.9
0.1

cm '
116


86.3
22.1
68.7
29.7
11.6
4.2
4.0
1.8
1.1

TOTALS              60.2   2.6   18.0   6.9   30.3   41.3   14.6   310.2   114.1   100.5   140.0   288.6   229.5

-------
 plot at the Gray site  that had never contributed percolate  during the study
 were excavated and brought back to the laboratory for analysis.   Leachate was.
 collected  by  the  extraction system  following water application to the
 lysimeter surfaces.   If the proper  amounts of irrigation  water had been
 available for application it is probable that more lysimeter units would have
 contributed percolate  during the study.

     The  depth of percolate  intercepted by the surfaces of the lysimeter
 units at the test sites  for  the two year study period are  shown  in Tables  16
 and  17.   The  amounts of water that were  applied through precipitation and
 wastewater irrigation  to the test  plots were  insufficient  to  generate  a pore
 volume  of percolate  in the volume of soil  over the  extraction assemblies  in
 the lysimeters. during  the study period.   The average porosities calculated
 from  soil measurements on  the Hancock and Gray sites were 0.458 and  0.451,
 respectively.  Using the average of these two values, a pore would contain  an
 average  of 27.7, 55.4,  and 83.2 cm  depths  of percolate  for  the tray
 lysimeters at  61,  122,  and 183 cm depths.   The four control  units and the
 122 cm tube 113, located next to a semi-permanent water puddle along the path
 of the traveling gun path on the bermu'da grass plot on the Hancock site, were
 the only units  that intercepted more  than a pore  volume during the test
 interval.

     The  amounts of percolate  intercepted by'all  lysimeter units with the
 exception of the tube  lysimeter on the control plot are small.   The values  of
 depth of percolate that  were recorded for both years are  not  indicative  of
 those that would be measured on  a  properly  operated  land application system.
 Much of the  percolate was  captured  during the winter and  spring when  no
 irrigation water was applied nor vegetative  growth occurring.  Percolate
 volumes and dates of percolate occurrence  at the different  profile leve.ls
 obtained  in  the study can  not  be  used to determine the  operational
.characteristics or the suitability of current design  criteria  for slow rate
 land  application systems  because of the inadequate hydraulic loadings that
 were realized.

     It is apparent  from the data  in  the tables that a wide variation  exists
 in the  number  of collection  events and the amounts of percolate collected
 between sites, among plots on the same site,  and between  units  on the same
 plot  and at the  same level.   Variations  in hydraulic loading rates between
 plots, in irrigation water applications  on the plot,   in soil properties above
 the lysimeter units, in  plot vegetation  and  cultural  practices,  operational
 characteristics of the individual  lysimeter  units, and operational procedures
 followed in operating  individual lysimeters  were factors  that caused the
 differences noted among  units in Tables  16 and 17.

 Percolate Quality

     The number of percolate collection  and  water quality sampling events for
 each lysimeter unit  over the project period are presented  in  Table 18.  Many
 of the  water  quality samples were  of such small  volume that only a few
 parameters could be  measured.   Also, the  timing  of the majority of the
 percolate collection events  was during the winter and spring months when
 vegetative growth was  minimal on the  test  plots and few  irrigation events

                                   61

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crv
                                                                             TABLE  16

                                                        DEPTH OF PERCOLATE INTERCEPTED BY LYSIMETER UNITS
                                                              OVER STUDY PERIOD AT THE HANCOCK SITE
Location
Tray
0.61 m



1.22 m



1.83 m



Tube
1.22 m


1.83 m


2.44 m

Controls
1.22 m


1.83 m


Bermuda
Units

101*
102
103 .
Avg.b
104
105
106
Avg.
107
108
109
Avg.

. HI
• 112
Avg.
113
114
Avg.



121
122
Avg.
123
124
Avy.
Depth
(en.)

5.1
12.2
4.4
7.2
0.9
1.2
Neg
1.1
0.3
4.1
—
2.2

—
0.1
0.1
108.1
43.1
75.6



171.3
155.3
163.3
113.3
114.9
114.1
Grain Sorghum
Units

201
202
203
Avg.
204
205
206
Avg.
207
208
209
Avg.

211
212
Avg.
213
214
Avg/
215
216
Avg.






Depth
(cm)

0.8
1.7
— — .
1.25
0.8
—
—
0.8
0.3
Neg
Neg
0.3

	
0.5
0.5
Neg
1.4
1.4
	
	







Cotton
Units

301
302
303
Avg.
304
305
306
Avg.
307
308
309
Avg.

311
312
Avg.
313
314
Avg.









Depth
(cm)

Neg
3.9
3.9
3.5
3.5
3.2
0.9
1.6
0.7
2.9
0.8
1.5

10.8
1.2
6.0
2.0
0.3
1.2









                            a(Jnit code In which the first digit identifies the plot and the next two identify lysimeter type and
                            depth.
                             Average of producing units.

-------
00
                                                                            TABLE 17

                                                        DEPTH OF PERCOLATE INTERCEPTED BY LYSIMETER UNITS
                                                               OVER STUDY PERIOD AT THE GRAY SITE
Location
Tray
0.61 m



1.22 m



1.83 m



Tube
1.22 m


1.83 m


2.44 ra


Bermuda
Units

101a
102
103 .
Avg.b
104
105
106
Avg.
107
108
109
Avg.

Ill
112
Avg.
113
114
Avg,
115
116
Avg.
Depth
(cm)

	
Neg
6.1
6.1
0.3
1.8
0.6
0.9
3.3
4.1
1.5
3.0

31.1
10.8
21.0
10.1
14.1
12.1
28.9
25.1
27.0
Cotton
Units

201
202
203
Avg.
204
205
206
Avg.
207
208
209
Avg.

211
212
Avg.
213
214
Avg.



Depth
(cm)

12.3
3.6
6.6
7.5
5.2
0.6
4.3
3.4
2.9
0.2
2.0
1.7

5.8
6.7
6.3
0.4
0.4
0.4



Grain Sorghum
Units

301
302
303
Avg.
304
305
306
Avg.
307
308
309
Avg.

311
312
Avg.
313
314
Avg.



Depth
(cm)

17.2
33.2
15.5
22.0
1.7
7.2
—
4.5
1.3
1.0
4.3
2.2

5.0
18.8
11.9
17.0
33.1
25.1



                            aUn1t code In which the first digit Identifies the plot and the next two Identify lyslmeter  type and
                            depth.
                             Average of producing units.

-------
                    TABLE 18

PERCOLATE AND WATER QUALITY  SAMPLING EVENTS FROM
       MAY 1, 1982 TO SEPTEMBER 30, 1983
Unit

101
102
103
104
105
106
107
108
109
111
112
113
114
115
116

101
102
103
104
105
106
107
108
109
111
112
113
114


121
122
123
124
Perc.

___
2
94
9
47
14
87
97
78
189
127
218
195
215
202

34
78
44
9
19 .
1
2
54
1
__
1
305
218


415
346
405
417
Qua!.

__
—
17
1
12
1
19
18
16
39
23
45
36
44
38

12
20
11
1
3
—
—
13
1
_
—
65
39


77
63
79
77
Unit

201
202
203
204
205
206
207
208
209
211
212
213
214



201
202
203
204
205
206
207
208
209
211
212
213
214
215
216




Perc.
Gray Site
94
59
119
55
8
16
74
9
14
ISO
93
17
5


Hancock Site
25
1
—
18
—
—
1
1
1
___
—
1
10
__
—




Qual.

15
5
19
4
—
1
2
1
—
29
13
2
—



5
—
—
2
—
—
__
_
—
__
—
_
2
_
—




Unit

301
302
303
304
305
306
307
308
309
311
312
313
314



301
302
303
304
305
306
307
308
309
311
312
313
314






Perc.

126
220
107
46
43
—
11
16
34
40
145
114
193



1
11
25
14
20
. 12
3
15
9
73
56
53
19






Qual.

21
42
17
• 8
5
—
3
2
4
7
26
21
41



__
3
12
3
3
• 1
2
1
4
17
11
13
3






                     64

-------
with wastewater effluent were occurring.

     The poor stands of cotton and grain  sorghum and the resulting  low yields
obtained on  the plots (Tables  19  and 20) during both growing  seasons
generally did  not represent conditions that would  occur  under normal
conditions in a municipal wastewater land application system.   Average yields
for  irrigated  cotton and grain sorghum in Lubbock county for 1982  and 1983
were 252 and  396 kg/cotton/ha and 3720 and 3390 kg/grain  sorghum/ha,
respectively (23).  Grain sorghum yields  at the Hancock site were higher than
the county average during both seasons.  The yields of bermuda  grass  were not
reported on a  county  basis.   Fertilization  with nitrogen  and  irrigation were
the primary determinants of yield with this crop (16).  Therefore, solute
levels  that were measured in the percolate samples collected from  the crop
plots during  the two growing  seasons covered in  the study  were  not
representative  of conditions where higher plant  densities per unit  area are
encountered.

     There is some benefit in comparing the composition of the  percolate that
was collected, even though the collection periods and the  less-than-normal
plant  populations  that existed on the plots were distorted, with  the
composition of  the  irrigation waters  applied  to the plot.   The solute
concentrations, of the percolate that  was intercepted had been impacted by
previous wastewater irrigation events on  the various plots.   The  geometric
mean (G), standard deviation (SD), number of sampling .events (E), coefficient
of variation  (CV),  percentage of composite samples (%C),  and the mass in
kg/ha for chemical constituents analyzed  in the quality samples obtained from
the lysimeters over the project period are shown  in Appendix D.  The mass in
kg/ha  was calculated using the geometric mean and the depth of  water
intercepted by the surface area of the lysimeter unit (Tables  16 and  17).

     The geometric means of  selected water quality  parameters  in  the
irrigation waters applied to the test areas are shown in  Table  21.  The
wastewater"quality applied at each site varied because of  the  different
treatment paths  at  the wastewater treatment plant,  sources of  wastewater
treated  in each treatment sequence,  and storage practices.   The water quality
characteristics of the water applied to the control plot were  obtained from
water sample analyses made at the municipal  water  treatment plant.

     Comparison of the  geometric  means of  the  constituent  concentrations
shown in Appendix D with those shown in Table 21 generally reveals  a  decrease
in nutrient levels  in the percolate samples.   Levels of total Kjeldahl
nitrogen (TKN), ammonia nitrogen (NH3-I\I),  total phosphorous  (TP),
orthophosphate  phosphorous (Ortho P),  and organic  phosphorous (Org.  P)
decreased by a factor of  10 or greater.   The levels of the combined  total of
nitrogen reported as nitrite/nitrate-nitrogen (N02+N03-N) increased in  the
percolate.  The  increase in  these forms resulted from the oxidation of the
other nitrogen compounds present in the applied wastewater as  well  as from
the mobilization by the percolate of nitrates stored in the profile.

     The cation and  anion concentrations as  depicted by  values of  the
geometric means of the collected percolate varied among similar  lysimeter
units at the same depth  level  on  the test plots and between the depth levels

                                  65

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                                        TABLE  19

                      CROP YIELDS AND GEOMETRIC MEANS OF SELECTED
                         PARAMETERS FOR TEST CROPS GROWN IN 1982
Site   Plot      Average Yield    Total        Total       Protein      Sulfur     Chloride
                              .   Nitrogen   Phosphorus
                 (kg/ha)a(%MC)b  (mg-N/g)    (mg-P/g)       (%)       (mg-S/g)    (mg-Cl/g)

Gray
   Berm. Grass    1.900  (68.3)   45.90

   Cotton0          0

   Gr. SorghumdfS 1.850  (33.5)   15.72

Hancock

   Berm. Grass    2,350  (74.6)   30.43

   Cotton0          6

   Gr. Sorghumd>e 9,760  (41.0)
3.14
3.02
3.04
28.22
 9.66
18.75
8.16
2,88
5.37
84.64
 1.30
 0.65
.Dry weight basis.
 Percent moisture at the time of harvest.
°.Stand too poor to harvest for reliable results.
 Unthreshed grain with approximately 10 percent stalk.
 Damage to grain from birds and/or insects.

-------
                                        TABLE 20

                       CROP YIELD AND GEOMETRIC MEANS OF SELECTED
                         PARAMETERS  FOR TEST  CROPS GROWN  IN 1983

Site Plot Average Yield Total
, Nitrogen
(kg/ha)a(%MC)b (mg-N/g)
Gray
Berm. Grass
ft
Cotton
d e
Gr. Sorghum '
Hancock
Berm. Grass
Cotton0
Gr. Sorghum

3,812 (68.2) 22.58
816 (43.1) 9.37
0 — 15.72

7.976 (67.7) 18.29
1,349 — 9.15
4.123 (14.1)
Total Protein Sulfur Chloride
Phosphorus
(mg-P/g) (%) (mg-S/g) (mg-Cl/g)

3.48 13.89 7.48 8.36
1.45 5.76 9.41 0.32
3.02 9.66 2.88 1.30

3.10 11.23 9.57 8.61
1.26 5.63 8.16 0.42
— —
• Dry weight basis.
 Percent moisture at the time of harvest.
.Stand too poor to harvest for reliable results.
 Unthreshed grain with approximately 10 percent stalk.

-------
                               .   TABLE  21

         GEOMETRIC MEANS OF  CONCENTRATIONS  FOR  QUALITY  PARAMETERS,
               IN  IRRIGATION  WATERS APPLIED  TO THE  TEST  AREAS
                          OVER THE PROJECT PERIOD .   .

PARAMETER
ALK
TDS
TKN
N02+N03-N
NH3-N
TOTAL P
ORTHO P
ORG P.
COD
Cl"
S04
Ca
Mg
K
Na
TOC
APPLIED
WASTEWATER
GRAY SITE
(mg/1)
295
1190
11:2
3.47
2.75
4.00
2.30
0.172
116.6
302
215
81.5
44.1
19.4
256
38.8
APPLIED
WASTEWATER
HANCOCK SITE
(mg/1)
347
1180
37.6
0.114
20.9
14.4
8.27
0.267
245
332
203
58.0
24.3
18.2
315
54.6
IRRIGATION
WATER
CONTROL PLOTS3
(mg/1)
200
924
-
' 0.109





247
181
47.1
23.3

223

Data compiled from records of Water Sample Analysis at the Lubbock
Municipal Water Treatment Plant.
                                     68

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on the same plot.  Differences were also  apparent among the  values for'the
same  constituent at the  same level between  plots.  The reasons for the
variation were  probably the same factors  listed previously for the  variations
in the amounts  of percolate collected.

     Sets of equivalent  ratios between the  meq/1  values for  cations and
anions  and indices calculated from groupings  of  meq/1 values  for these
parameters were developed where data was  available using the geometric means
of the  percolate,  applied irrigation waters,  and underlying  ground water at
each site.  Insufficient  data at the Hancock site limited  the  number of
values obtained.  The ratios for the various plots are shown in Tables E-1 to
E-6.   The values used for the ground water at the Hancock site were geometric
means developed from data  taken during the  baseline period (June 1980 to
February 1982)  before wastewater was applied.

     The majority of the. values developed from  the percolate  data are less
than  1.   Normally,  in  soils containing  high levels of  carbonate, the
equivalence ratios are higher than unity  (11).  The values exhibited at all
sites are an  indication of the impacts  from relatively higher levels of Ma,
Cl, and  HC03 in the irrigation water.

     The adjusted SAR values (1) exhibited for  the applied waters on all test
areas were sufficient  to cause impacts on  the soil  in  the  form of
deflocculation of clays,  reductions  in infiltration rates and  decreases in
the availability of K.  Additionally,  the  high  SAR values  found in these
waters  were sufficient to  cause phototoxicity of the- test  crop  plant  leaf
surfaces and to pose difficulties in root  absorption of the  soil waters
resulting from irrigation using these waters.  The high value (20.1) of the
adjusted SAR of the wastewater effluent applied at the Hancock  site can be
expected  to cause the rapid  development of  soil and crop problems at that
site.   The adjusted SAR values for the ground water at the Gray site are much
higher as a result of the long history of wastewater irrigation, than those
determined for  the ground water at the Hancock  site.

     The adjusted SAR ratios for the percolate at the Gray site  were greater
than the values for the irrigation water  and the ground  water.  All  values of
the adjusted  SAR at the  Gray site indicate  root  adsorption problems.
Adjusted SAR values for the percolate at  the Hancock  site (Tables E-4 through
E-6) are lower  than those obtained for either the applied water or  the ground
water.   These  lower values indicate that adsorption and retention of Na was
occurring in the profile.   The values for the two control  units were slightly
higher than those calculated for the other units irrigated with wastewater.

     Base exchange indices (IBA) given by Schoeller (14) in Mathess (11) were
calculated for  the applied water,  percolate,  and  ground water.  A positive
index is an indication of favorable conditions  for an exchange of alkalis (Na
and K) in the  water  for alkaline earth ions (Ca and  Mg) in the soil  (11).  A
negative value  of the index indicates favorable conditions for the exchange
of alkaline earths in the  water for alkalis in the soil.   The positive value
of the  IBA  values  for the  percolate  intercepted  by  the majority of the
lysimeters indicated that alkalis in the  soil  water  were  being exchanged for
Ca and Mg in the root zone.

                                   69

-------
     The (C1~ - Na+)/Cl~ index also  establishes the value of  the sign for the
IgA.  The high sodium content of the applied waters is seen  by the  negative
values  obtained  for this  number.   This indicator is also  negative for the
ground water at both sites.   Negative values of (Cl~ - Na+)/Cl~ and  Ig/\  are
seen  for percolate at four  locations  (3 tubes and 1 tray unit)  at the Gray
site.   Percolate at 11 locations exhibited positive values.

Mass Transport Results for Percolate Flows

     Tables  F-l to F-7 show the masses of the parameters that were  measured
in  the  quality  studies of the applied  irrigation water and  of the percolate
intercepted by  the lysimeters during the project period.  The  average
geometric mean of the parameter at the profile depth and the  average depth of
water calculated  from the contributing lysimeters on the plot at that level
were used to calculate the values shown.  The seven tables also present the
masses of various  constituents  that were contained in crops  produced on each
plot;  these  were calculated from sample  analysis and crop production  figures
for the two  crop  seasons.   The  crop  production figures for the two sites are
given  in Tables 19 and 20.

     The mass values calculated for the control,  plot show  close agreement
between  applied  amounts and mass transported by the percolate.   This was to
have been expected with the loading  applied on the control  units.   On the
other plots, the parameters that may fall within a factor of 10  of the
applied  rates were alkalinity, TDS,  Cl,  and the cations.  Tables  F-l  to F-7
indicate that even with the deficits experienced  .in hydraulic loading on the
test plots the translocation of large amounts of material (Na, Ca,  Cl,  SOM
and alkalinity)  occurred  at different depths in the profile.  Movements of
the magnitudes shown in these tables may impact the quality  of ground  water
under  these  sites  if  irrigation  is continued  at design rates on the sites in
the future.

SOIL ANALYSIS

    The soils at both  sites  generally  followed  the  typical  profile
description presented in  Appendix A.   The layers of calcium  carbonate,
regionally referred to as caliche,  varied in  thickness, cementation,  and
hardness within the plots,  between the plots,  and between  sites.   A layer of
indurated caliche was generally found at each  site between  45 and  183 cm.
This condition was more pronounced in  the Friona soils at the Gray site.

     In   addition to the  variability of those soils formed from  eolian
sediments, it was noted during excavation made for the percolate  extraction
facilities  that  the Hancock test  area had previously been the site of a
prairie  dog  colony.  The burrows had  subsequently filled with surface soil
over a  time interval.  The  walls  of each of the three excavations showed
evidence of  the old burrows  through color differentials exhibited  by the
darker  surface  soils occupying the old burrows in the lighter colors of the
undisturbed  materials in the lower horizon.   The  burrows noted were  within
240 cm of the soil surface.

    An  examination  of  constituent  changes  in  the  soil between  sampling

                                   70

-------
intervals  is  presented in this  section.  Accumulations and depletions  at
different  depth levels were noted  in the same profile for many materials.
Table 22 shows  the  variability that existed  for selected  cations and anions.
Sodium  and chloride increases  are  noted on all plots  at  the Hancock site,
whereas  depletions of both materials are noted in the majority of the  depth
intervals  at  the Gray site.  The levels of N02+N03-N decreased in all levels
on the plots  at  the  Hancock sjte.  The effects  of the  low hydraulic loadings
on this  constituent  can be seen on the cotton and grain  sorghum plots at the
Gray site.    .                                                    _

Nutrients

     An  examination  of the variations  of nitrogen compounds at both sites  at
30-cm increments was made down to the 90 cm depth for the sampling events  in
the springs of 1981 and 1983,  and in the fall of 1983.  The  caliche layers  at
the Gray site required that the  soil from 90 to 180 cm depth be composited.

     The average values for the depth  intervals at each  sampling period show
a decrease in  TKN (Table 23) with  depth.   Based  upon the levels of NH^-N
shown in Table 25 for the depth  intervals in these soils,  the TKN  for the
sites was  judged to be primarily  organic nitrogen.  Although there was little
difference in  the TKN measured at the two sites, the average values in the
profile  at  the Hancock site were higher (4.6  mg N/g  compared to 4.1  mg N/g).
This would  amount to a difference of 0.5 kg N per metric ton of soil between
the two  sites or 1400 kg N/ha in the  top meter  of soil,  with an average bulk
density  of 1.4  g/cm3.  With the exception of the cotton  plot, examination  of
the average values in the profile for  the plots at the Hancock site to the  90
cm depth showed  a general  decrease  in  TKN during  the study period.   At the
Gray  site,  the  average TKN of  the  three plots at the  90  cm depth for each
sampling period  showed little change.   Three  of the plots (the bermuda grass
and the grain  sorghum plots at  the Hancock site, and the cotton plot at the
Gray  site) exhibited their lowest  values of TKN  during  the March 1983
sampling period.

     The N03 -N  content in  the  soil profiles at the Hancock site were
generally  higher both at the start  and end of  the project than were the
levels  measured at the Gray site (Table 24).   The  average  profile N03-N
content  for the  three sampling  periods in the  top 90 cm showed a  general
decrease  over  time.  High  concentrations of  nitrates were found  in the
initial percolate volumes  intercepted  by  many  lysimeter  units.
Concentrations generally decreased  as  the volume of flow  recorded increased.

      Again,  the NH3-N data in Table  25 show that larger initial values were
present  in  the soils at the  Hancock site.  Generally, decreases of NH3-N  in
the profile  occurred over the  project interval.  Also noticeable over the
three project  periods was the  decrease of NH3-N  with depth.   The  grain
sorghum plot on the Gray site  exhibited the  highest  value in the  90  cm
profile  during the spring of  1983.

     Table  26 shows the total  phosphorous present in the  upper 91 cm  of the
soil  profile in the three sampling  periods during the study.  The profile
averages for  the last sampling event show that decreases  in  total phosphorous

                                   71

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                               TABLE 22

CHANGES IN 10~2 mg/g OF SOIL WITH DEPTH FOR SELECTED CATIONS AND ANIONS
       BETWEEN SAMPLING PERIODS IN MARCH 1981  AND NOVEMBER 1983.

Plot

Bermuda



Cotton



Grain
Sorghum .




Bermuda





Cotton





Grain
Sorghum





Depth
.Interval
(cm)

0-30
30-60
60-90
90-180
0-30
30-60
60-90
90-180

0-30
30-60
60-90
90-180

0-30
30-60
60-90
90-120
120-150
150-180
0-30
30-60
60-90
90-120
120-150
150-180

0-30
30-60
60-90
90-120
120-150
150-180
Na

-8.2
-8.0
-52.3
-8.5
-8.4
-1.1
10.7
-.5

-11.8
-13.7
-11.7
9.4

4.4
9.5
3.6
-0.1
0.3
-8.3
27.4
53
83
-4.6
-6.4
-9.9

17.6
16.7
2.0
410
12.0
-7.8
Ca
Gray Site
15,780
.3,460
14,200
7,750
-6.0
-79.0
-384
10,900

223
-116
-47.0
4,010
Hancock Site
1,800
606
-490
14,100
6,940
15,200
-10.9
-12,100
-833
6,570
9,200
6,790

11
-346
-40
-3,480
10,300
12,500
Cl

-2.0
-8.4
1.1
-4.2
-2.8
9.8
3.8
-0.3

-2.5
-6.1
-4.7
-0.8

1.8
4.2
4.7
7.4
13.0
13.4
15.2
-3.3
-1.0
0.5
3.6
-1.4

0.7
7.6
8.7
1.2
-0.2
-3.8
so4

-8.4
-1.5
15.0
-194.2
-4.1
-205
-204
-161

-231
-204
-204
-194

-1,7
4.1
8.4
-7.7
-6.6
-2.2
-3.5
3.8
10.3
9.3
6.7
6.5

-5.9
-1.9
-0.7
-3.2
-4.6
-4.2
N02«03-»

-1.45
-1.00
-0.33
-0.35
-1.00
0.18
0.94
0.94

-0.29
0.34
-0.09
0.82

-0.29
-0.60
-0.94
-3.75
-0.76
-1.22
-0.43
-0.89
-0.93
-0.78
-0.72
-0.76

-0.04
-0.34
-0.43
-0.68
-0.05
-0.03
                                 72

-------
co
                                                                                  TABLE  23
                                                                RESULTS OF  SOIL ANALYSIS  FOR  TKN-N ON TEST PLOTS
                                                                  FOR  3 SAMPLING  PERIODS  IN 10'1 mq/q OF SOIL
Site Depth
(">)
Hancock 0 - .30
.30-. 61
.61-. 91
Avy. In
profile
Gray 0 - .30
.30-. 61
.61-. 91
• Avg. in
profile

3-4/81
6.1
5.8
7.8
6.6
5.2
2.8
2.2
3.4
Bermuda
Plot
2/83
5.6
4.6
3.2
4.5
5.0
3.8
2.2
3.7
Grain Sorghum
Plot
11/83
6.6
4.9
2.6
4.7
5.4
3.7
1.1
3.4
3-4/81
5.5
5.0
2.6
4.4
6.3
4.1
2.5
4.3
2/83
. 4.0
3.9
2.4-
3.4
5.0
5.2
4.8
5.0
11/83
5.3
4.9
2.7
4.3
4.8
3.6
2.7
3.7
3-4/81
4.4
4.4
3.3
4.0
6.4
3.9
2.8
4.4
Cotton
Plot
2/83
6.0
5.5
3.2
4.9
4.8
2.6
2.8
3.4
Avg. in Depth
Interval
11/83
5.2
5.4
2.7
4.4
6-7
5.0
3.6
5.1
3-4/81
• 5.3
5.1
4.6
5.0
. 6.0
3.6
2.5
4.0
2/83
5.2
4.7
2.9
4.3
4.9
4.0
3.3
4.1
11/83
5.7
5.1
2.7
4.5
5.6
4.1
2.5
4.1

-------
•-J
4=.
                                                                                      TABLE  24
                                                                   RESULTS OF SOIL ANALYSIS  FOR NO-j -N ON TEST PLOTS
                                                                      FOR 3 SAMPLING  PERIODS IN 10'3 mg/g OF SOIL
Site Depth
(m)
Hancock 0 - .30
.30-. 61
.61-. 91
Avg. In
profile
Gray 0 - .30
.30-. 61
.61-. 91
Av9. (n
profile

3-4/81
3.35
6.32
9.80
6.48
14.71
11.72
5.04
10.47
Bermuda
Plot
2/83
2.21
1.64
0.44
1.42
1.42
.14
1.11
0.84
Grain Sorghum
Plot
11/83
0.44
0.36
0.40
0.40
2.28
1.72
1.72
1. 90
3-4/81
7.85
7.93
6.24
7.34
15.38
0.32
0.34
5.34
i/83
4.01
3.52
3.26
3.59
1.72
7.74
6.60
5.35
11/83
7.47
4.54
1.90
4.63
2.15
1.28
1.26
1.56
3-4/81
6.37
10.57
12.12
9.68
6.49
1.19
4.99
4.22
Cotton
Plot
2/83
2.64
3.19
2.04
2.62
2.76
2.13
6.97
3. 5
Avg In Depth
Interval
11/83
2.04
1.67
2.83
2.17
1.53
0.58
0.56
0.89
3-4/81
5.85
8.26
9.38
7.82
12.18
4.41
3.46
6.67
2/83
2.94
2.78
1.91
2.54
1.96
3.33
4.89
3.39
11/83
3.31
2.19
1.71
2.40
1.98
1.19
1.18
1.45

-------
                                                                                  TABLE 25
                                                            RESULTS OF  SOIL  ANALYSIS FOR N»3-N ON  TEST  PLOTS
                                                               FOR 3 SAMPLING PERIODS IN IP'3  mg/g OF SOIL
cn
Site Depth
•(•)
Hancock 0 - .30
.30-. 61
.61-. 91
Avg. in
profile
Gray 0 - .30
.30-. 61
.61-. 91
Avg. In
profile

3-4/81
1.22
1.72
3.11
2.01
2.61
0.44
1.17
1.40
Bermuda
Plot
2/83
3.46
1.36
0.87
1.89
1.85
0.86
0.56
1.09
Grain Sorghum
Plot
11/83
0.25
0.60
1.06
0.63
1.57
0.82
0.57
0.99
3-4/81
3.31
2.42
1.66
2.46
2.46
1.16
0.73
1.45
2/83
1.38
2.44
1.36
1.72
1.40
1.44
2.73
1.85
11/83
1.18
1.17
0.63
0.99
2.15
1.28
1.26
1.56
3-4/81
2.47
1.85
1.35
1.89
2.89
0.76
4.38
2.67
Cotton
Plot
2/83
1.10
0.80
0.71
0.87
1.89
2.13
3.87
2:62
Avg In Depth
Interval
11/83
1.17
0.69
0.94
0.93
1.53
0.58
0.56
0.89
3-4/81
2.33
1.99
2.04
2.12
2.65
0.88
2.09
1.87
2/83
1.98
1.53
0.98
1.50
1.71
1.48
2.38
1.85
11/83
0.86
0.82
0.87
0.85
1.75
0.89
0.80
1.15

-------
(ft
                                                                            TABLE 26
                                                 RESULTS OF  SOIL ANALYSIS  FOR  TOTAL PHOSPHORUS-P ON TEST PLOTS
                                                           FOR  3 SAMPLING PERIODS IN 10-1  tng/g OF SOIL
--------- - - - . - _ _ III __
Site
Hancock


Gray


Depth
(.11)
0 - .31
.31-.61
.61-.91
Avg. In
Profile
0 - .31
.31-.61
.61-.91
Avg. in
Profile
Bermuda
Plot
3/81
1.2
2.2
1.9
1.77
2.3
2.1
4.0
2.80
2/83
1.9
2.0
1.8
1.9
4.0
2.4
1.3
2.56
11/83
1.5
1.6
1.6
1.57
1.7
4.2
3.6
3.16
Grain Sorghum
Plot
3/81
1.3
1.3
1.6
1.40
5.9
2.1
1.8
3.26
2/83
1.4
1.9
2.1
1.8
4.6
2.9
3.0
3.5
11/83
1.4
1.4
1.3
1.37
4.2
2.5
2.8
3.16
3/81
1.0
1.6
1.7
1.43
4.9
2.7
2.3
3.30
Cotton
Plot
2/83
1.3
1.6
1.6
1.5
4.8
2.7
3.2
3.57
11/83
1.5
1.5
1.3
1.43
4.7
2.6
2.4
3.23
Avg. In Depth
Interval
3/81
1.17
1.70
1.73
1.53
4.37
2.3
2.7
3.12
2/83
1.53
1.83
1.83
1.73
4.47
2.67
2.5
3.21
11/83
1.47
1.5
1.4
1.46
3.53
3.1
2.93
3.19

-------
occurred in  four of the plots.  An increase  in total phosphorous  was observed
at the profile  at the  bermuda grass plot on  the Gray site.   No  change in
average profile content was observed between the first and  last  reading made
on the cotton plot at  the Hancock site.   A rise in the average  profile total
phosphorous  content was noted for all plots except the bermuda  grass  plot at
the Gray site.  The average values observed  for the profile  at  the  Hancock
site at the end of  the project  were  approximately 50 percent  of these at the
Gray site.

     Table 27  shows  the  orthophosphate phosphorous  in the  three 30  cm
increments  of the upper soil profile  of  the  plots.  At the end of the  project
period,  the  available soil  phosphorous was  two orders of magnitude  less on
the bermuda  grass and  the grain  sorghum  plots  at the Hancock site than the
values  obtained on the companion plots at  the Gray site.   Orthophosphate
phosphorous  in  the cotton plot at the Hancock  site, however, was  one order of
magnitude less  than what was recorded at the Gray site.   Examination  of the
average  values in  the profile show that  orthophosphate phosphorous levels
decreased over  the project period in  the upper 90 cm depth at  both  sites.

Priority Organics

     The composition of the project  soils at  the beginning  and. end  of the
project period  showed  reductions in most of  the  priority organics measured at
both sites.  The location of the 20 materials  identified in the project soils
in November 1983  and the maximum levels of each compound,  in ppb, are shown
in Table 28.  Thirty-six organic compounds were  identified  in project soils
in analyses  performed in the spring of 1981.   Reduction in concentration of
11 of the organics found  in  November  1983 had occurred over  the  project
period.   Increases had occurred in the concentration of  nine  compounds:
carbon .tetrachloride,  dibutylphthalate,  hexadecane, methyl heptadecanoate,
methyl hexa-decanoate, octadecane, phenol, propazine, and tetrachlorethylene.
The greatest  increase  in the soil profile occurred in the  levels  of carbon
tetrachloride, hexadecane,  and dibutylphthalate.  The two former compounds
are solvents.   The mass  loadings  in  kg/ha  applied  to the  irrigation
wastewater  over the project period for  these  three materials  were  calculated
for the bermuda plots  at both sites because  of the higher hydraulic loadings.
The mean concentrations  and mass loadings  of those  substances  in  the
wastewaters  going to the Hancock site during .the project period  were 5.8 yg/1
for carbon  tetrachloride (0.145  kg/ha);  2.0  yg/1 for hexadecane  (0.05  kg/ha);
and 104  yg/1  for  dibutylphthalate (2.6 kg/ha).  In water going to the Gray
site the values were 4.7 yg/1 for carbon tetrachloride (0.066 kg/ha)  and 140
yg/1  for dibutylphthalate (1.98 kg/ha).   Hexadecane levels were not
determined  for  the treated effluent transported to the  lagoon  on the  Gray
site.

Trace Metals

     A mass balance  of the metals  in  the  soils of each plot was developed
using the soil  analysis data that were taken at the  beginning and end of the
project for each 30 cm depth  of  soil down to  183 cm.  The mass  of  each 30 cm
layer was determined from measured bulk  density values that  had been made.
The net  change in  the metal  content in mg/kg was then used to determine the

                                    77

-------
00
                                                                           TABLE 27
                                                  RESULTS OF SOIL ANALYSIS FOR ORTHOPHOSPHATE-P OH TEST PLOTS
                                                          FOR 3 SAMPLING PERIODS IN 10~3 mg/g OF SOIL
___ 	 -- -1- - _ ._.
Site
Hancock


Gray


Depth
(n.)
0 - .31
.31-.61
.61-.91
Avg.ln
Profile
0 - .31
.31-.61
.61-.91
Avg. in
Profile
Bermuda
Plot
3/81
1.97
1.01
0.64
1.210
17.36
15.76
4.25
12.46
2/83
0.02
0.08
0.02
0.04
7.20
6.64
0.02
4.62
11/83
0.04
0.01
0.06
0.037
6.84
4.68
.02
3.85
Grain Sorghum
Plot
3/81
2.47
1.05
1.05
1.523
16.78
24.35
19.69
20.27
2/83
0.02
0.02
0.02
0.02
1.88
19.44
13.76
11.69
11/83
0.08
0.05
0.05
0.060
5.99
9.44
13.47
9.63
Cotton
Plot
3/81
1.69
1.55
1.05
1.430
33.27
34.14
30.90
32.77
2/83
0.38
0.13
0.13
0.213
1.69
1.97
1.25
1.64
11/83
1.35
0.02
0.02
0.463
6.88
5.90
1.19
4.65
Avg. in Depth
Interval
3/81
2.04
1.20
0.91
1.38
22.47
24.75
18.24
21.82
2/83
0.14
0.08
0.06
0.09
3.59
11.56
5.01
6.72
11/83
0.49
0.03
0.04
0.19
6.57
6.67
4.89
6.04

-------
ID
                                                                            TABLE 28

                                                     MAXIMUM CONCENTRATION  IN PPB AND LOCATION OF ORGANICS
                                                       IN THE  SOIL PROFILE AT TEST SITES IN NOVEMBER 1983
Hancock Site

Anthracene/phenanthrene
Atrazlne
Benzene
Carbon tetrachlorlde
Chloroform
1-chlorotetradecane
Dibutylphthalate
Olchlorobenzene
Ethyl benzene
Heptadecane
Hexadecane
Methyl heptadecanoate
Methyl hexadecanoate
2-methylphenol ,
4-methyl phenol
Octadecane
Phenol
Propazi.ie
Tetrachloroethylene
Trichloroethylene
0-0.3
(rn)
1.6
89
6.0
4.2 •
1.8
50
1110



350





36.8
141
4.5
1.4
0.3-0.6 0.6-0.9
(m) (m)
5.4

3.7 1.6
3.1 2.1
1.1
82 6.2
890 140
16 -
1.4
81 170
460 1150
224



34 102


2.9 2.0

0.9-1.2 1.2-1.5
(m) (m)
41
74
1.0 1.0
2.5 2.5

71
150 •


115
340 260

280


70


2.6 1.5

Gray Site
1.5-1.8 0-0.3 0.3-0.6 0.6-0.9 0.9-1.8
(m) (rn) (m) (m) (m)


1.0 1.4 1.6 1.1 1.2
3.7 3.2 2.8 2.9 2.8


40 40


39
300 200 200 280 210


14 22
13

1.9

2.0 36 2.5 3.1 2.8


-------
mass change in  each layer and these values were summed over the 183  cm depth.
The results of  this are shown in Tables  29 and 30.

     The input  of metals  to  each plot was  determined from  the  amounts of
wastewater applied on  each plot and the geometric mean  of the quality
characteristics of the applied water.  The changes in the  soil  profile were
greater than  had  been anticipated  from the application  rates of the
inorganics.  In some  instances, such as  with sodium,  the  response was within
the same order of magnitude.  For most of  the heavy metals,  however, a much
larger accumulation is shown  in the soil data than would  be warranted by the
application  rates  utilized.   Provided the data  were  correct,  the.
accumulations or depletions such as those shown  in Tables  29  and  30 are of
definite concern.   Variability in soil properties from site to  site on the
test plots, even when composite samples  were analyzed, introduced errors that
could not be eliminated unless a much  larger  number of  samples,  randomly
collected from  the plot,  were to have been  analyzed.   Extrapolation of these
results,  using  the bulk densities to determine  soil mass,  also contributes
errors in the results.

Bromide

     Soil  cores to  be  analyzed for  bromide were taken on each test area in
March and November 1983.  The  results of the analysis are  shown in  Tables 31
and 32.                        '

1982 Crop Season—
     The two plots at the Hancock sites  which received the greatest  hydraulic
loading  contained little residual bromide in the 183 cm deep profile.  The
grain sorghum site received a hydraulic  loading 66.4 percent as great as that
applied on  the  cotton site and 38.5 percent  as great as that  on the bermuda
grass  (Table  12).   It appeared from the profile data shown in Table 31 that
the bromide moved about 1.5 cm down through  the profile for each  centimeter
of water applied at this site.

     Variability in movement  was much greater at  the  Gray  site.  The bermuda
plot,  with  a much larger hydraulic  loading (Table 11), showed  a bromide ion
accumulation in the 60 to 90 cm level.   This corresponded  to the depth of the
indurated  caliche layer that was encountered in placing the tray  lysimeters.
Moreover, this  level  occurred  in the region of maximum moisture content that
had been identified in the soil profile  with the neutron probe.  The movement
of bromide  on the other two plots was  approximately 1.95 cm per centimeter of
applied water.

1983 Crop Season—
     The general movement rates  exhibited during the 1983  crop season are
presented in Table 32.  The hydraulic  loading during  the  interval  was less
than that  shown  in  Table 31  because of the time period difference between
analyses.   The  cotton and grain sorghum  plots still had bromide  present in
the surface layer.   Some translocations  were evident in the bermuda plots
because of  the  heavier hydraulic loading on  these plots (Tables 13  and 14).
At  the Gray  site,  the effect of the caliche layer on the bromide was
evidenced by build-up of  bromide in the 45 to 60 cm layer  on the bermuda

                                    80

-------
GO
                                                  TABLE 29

                          APPLICATION OF  METALS  IN  WASTEWATERS  AND  FATE  OF  METALS
                              IN PLOT ROOT ZONE OVER PROJECT PERIOD—GRAY SITE

Bermuda
Metal
Al
As
Ag
Ba
Cd
Co
Cr
Cu
Fe
K
Mg
Mn
Na
N1
Pb
Zn
Applied
in
irrigation
kg/ha
1.550
0.098
0.078
5.460
0.031
0.095
0.973
1.590
7.500
530.000
442.000
0.528
3730.000
0.189
0.111
1.570
Awt in
profile
1000
kg/ha
141.000
-0.056
4.000
2.470
0.016
0.212
0.089
-0.345
-66.600
-47.000
-15.100
-1.620
0.323
-0.170
-0.016
-0.272
Cotton
Applied
in
irrigation
kg/ha
0.573
0.036
0.029
2.020
0.012
0.035
0.360
0.587
2.770
196.100
164.000
0.195
1380.000
0.700
0.041
0.582
A wt in
profi le
1000
kg/ha
105.000
0.128
0.003
-1.730
0.005
0.126
-Q.301
-0.047
-0.180
-28.100
8.640
-1.400
0.031
-0.089
0.008
-0.088
Grain Sorghum
Applied
in
irrigation
kg/ha
0.665
0.042
0.034
2.340
0.014
0.041
0.418'
0.681
3.220
227.000
190.000
0.227
1600.000
0.810
0.047
6.780
Awt in
profile
1000
kg/ha
-22.500
0.062
0.007
-0.595
0.009
0.098
0.414
-0.005
47.800
-12.700
1 1 . 300
-2.640
-0.614
-0.420
-0.008
-0.463

-------
00
                                                TABLE 30.

                         APPLICATION OF METALS IN WASTEWATERS AND FATE OF METALS
                           IN PLOT ROOT ZONE OVER PROJECT PERIOD—HANCOCK SITE

Bermuda
Metal
Al
As
Ag
Ba
Cd
Co
Cr
Cu
Fe
K
Mg
Mn
Na
Ni
Pb
Zn
Applied
in
irrigation
kg/ha
1.910
0.157
0.125
5.170
0.300
0.125
1.580
0.894
18.800
820.000
741.000
0.580
5990.000
0.462
3.250
3.910
Awt in
profile
1000
kg/ha
43.200
0.349
0.219
0.419
0.008
0.117
0.497
0.054
64.400
-13.400
12.800
-0.892
2.110
-0.201
-0.201
-0.806
Cotton
Applied
in
irrigation
kg/ha
1.070
0.088
0.070
2.900
0.168
0.070
0.884
0.502
10.540
460.000
416.000
0.326
3360.000
0.259
1.820
2.190
Awt in
profi le
1000
kg/ha
-67.200
0.435
0.099
0.726
0.007
O'.OSO
0.470
0. 934
29.100
-18.400
7.000
-1.640
0.848
-0.031
-0.069
-0.628
Grain Sorghum
Applied
in
irrigation
kg/ha
0.443
0.036
0.028
1.170
0.068
0.028
0.358
0.203
4.270
187.000
168.000
0.132
1360.000
0.105
0.738
0.889
Awt in
profile
1000
kg/ha
28.600
0.750
0.020
0.777
0.030
0'.125
0.710
0.627
51.900
-5.070
13.000
-1 . 300
1.930
-0.016
-0.016
-0.545

-------
00
CO
                                                     TABLE  31

                               BROMIDE TRACER LOCATION IN PLOT SOILS IN MARCH 1983
                                          AFTER APPLICATION IN MAY 1982

Concentration in mg/q at depths below surface
Sample
No.
XI 98
X202
X203
XI 99
X200
X201
Plot
Hancock 2 Grain Sorg.
Hancock 1 Bermuda
Hancock 3 Cotton
Gray 3 Grain Sorghum
Gray 1 Bermuda
Gray 2 Cotton
0-15 cm
<0.0002
<0.0002
<0.0001
<0.0002
<0.0002
<0.0001
91-102 cm
0.324
<0.0001
<0.0001
<0.0001
2.288
<0.0001
122-132 cm
4.322
<0.0002
<0.0002
<0.0002
<0.0002
1.132
168-183 cm
1.619
<0.0001
0.487
2.255
<0.0001
1.809
              Detection Limits = 0.1  mg/1  in extract
                                 or
                                 <0.0001 mg in 100 g of soil
                                 <0.0002 mg in 50 g of soil

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                       TABLE 32

BROMIDE TRACER LOCATION IN PLOT SOILS IN NOVEMBER 1983
            AFTER APPLICATION  IN MAY 1983

Sample
No.
X198
X202
00
** X203
XI 99
X200
X201
Plot
Hancock 2
Grain Sorg.
Hancock 1
Bermuda
Hancock 3
Cotton
Gray 3
Grain Sorg.
Gray 1
Bermuda
Gray 2
Cotton

0-15 cm
.0094
.0050
.0100
.0051
.0054
.0051
Concentration in mg/g at
30-45 cm 45-60 cm 60-75 cm
<.0002 <.0002
.0029 .0254
.0059
<.0002 .0036
.0067 .0107
.0108 .0036
depths below surface
75-91 cm 91-107 cm 168-183 cm
.0037
<.0002 . .0057
.0044
.0029 .0032
.0181 .0049
.0032

-------
plots similar  to  that shown in Table 31  for 1982.  The cotton  plot, with a
greater  hydraulic loading  than the grain sorghum plot, showed an  increased
bromide  content in the 30  to  35 cm layer.

FIELD USE OF EXTRACTION LYSIMETERS

     Employment of  lysimeters  in  the soil  root  zone  to monitor percolate
generated in the land treatment  of  municipal wastewater  is  an attractive
concept for improving system management.  .Detection of undesirable pollutant
concentrations  in  percolate would  signal  a need to initiate  operational
changes to reduce the application of the problem pollutant or pollutants.
With present monitoring techniques,  pollutants are  not detected until  ground
water samples  from monitoring  wells  reflect compositional changes.  By the
time pollutants  are detected in ground  waters, large amounts  of  the
contaminating substance may be in transit  both in the unsaturated zone and- in
the  saturated  zone.  Early warning  by  detection of potential  pollution
problems in the root zone  would reduce environmental impacts  on  area  ground
waters.

     The extraction  lysimeter  systems utilized  in  this study to  sample
conditions -in  the vadose zone  are  not,   however,  suitable  for  use  as
monitoring devices in land  treatment of municipal wastewaters.   The  primary
probTem  is the high cost associated with the collection of  useful  data  from
extraction lysimeter systems.

     Specialized equipment  is  required to  prepare  and emplace  lysimeter
systems.  Support facilities for  controlling lysimeter conditions  and
percolate collection must be installed.   Because  soil property  differences,
either in the undisturbed  core of the tube  lysimeters or  in the  undisturbed
soil layers overlying the tray lysimeters, affect  the rates  of percolate
movement, percolate volumes and the composition of  percolate,  the lysimeters
must be  operated continuously.  If information useful in the operation of the
land treatment  system is to be obtained, frequent data collection  and sample
analysis will be required.   Useful  information can be  obtained  about the
impacts of biological  activities  on  soil water flow  using either the
extraction or weighing type of lysimeter.   In the  author's opinion, however,
there is a question now, after completion of this study, as to whether any
lysimeter system can reproduce the conditions of soils in their natural state
or can detect the subtleties  inherent in the hydraulic response  of soils in
the natural state at a specific location.

     Study  results  indicated  that  percolate  moves  through the  profile in
erratic and unpredictable sequences.  Even on  the  control plots,  where
application of water occurred at a frequent and sufficient rate to maintain
soil moisture conditions at levels at which  percolate flow was  continuous,
the  arrival of the peak rates  of flow at  the collection unit varied over a
range of 1-to-3  days after an irrigation event.   Additionally,  the
variability of soil properties over the  site and vertically in the  profile
affects  percolate volumes  and characteristics.  This situation was  noticeable
in study results and dictates that replication of lysimeter  units must be
provided at the  site in future studies  if reliable information is to be
obtained.  All of these factors add to the costs associated with the  use of

                                   85

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extraction lysimeters.

     The attention  and  expense required  to  operate  lysimeters in the  root
zone limit their applicability to research activities rather than operational
management of  land treatment systems.  Lysimeters can be useful in helping to
define what occurs in the root zone.   The two  types  of  units used on the
project would require modifications in system component construction and in
the test  environment if they are  to be  employed  in another  research
application.   Problem areas  with ihe lysimeters utilized in the study  that
require consideration before employment in future  research efforts are
presented  in the following lists.

Tray Lysimeters

     1.   The  auger  used  to drill the pilot hole for the cavity would drift.
This produced  a dome-like roof area  for a portion of the  cavity in a few
locations  where vertical  drift occurred.

     2.   The small  cavity opening made it difficult  to determine the shape
of the roof area at greater  distances  from the  manhole.  The inability to
examine roof  shape  thoroughly can result in conditions where no contact is
made between the soils in the  tray and those in the roof surface.

     3.   Puddling  of the  soil in the  cavity walls  occurred during the
forming, of the  final rectangular shape of the tray  cavity.  The back-and-
forth movement of the cutting  head  along the soil surface  compressed and
smoothed  the  surface zone.   Packing  of this  surface could decrease the
hydraulic  conductivity of the  soils in the roof area in contact with the  soil
surface of the tray and  thus  produce  a soil condition  less conducive to
percolate  flow.

     4.   Techniques to  better position the tray surface against the cavity
roof need  to be developed.  The positioning of the trays to  obtain suitable
contact with  the  roof surface was finally accomplished by means of wooden
wedges.   The  additional movement and  vibration of  the trays during the
interim could  have caused both spalling  of  the  roof soil and spillage of the
tray material, thus resulting  in less contact between the two surfaces.

     5.   Improvement is  needed both in the materials used in wick assembly
and in the techniques of  their construction.   Aging of the materials used in
forming the connective  joints between  the ceramic  candles in  a moist
environment may  have caused  the further deterioration  in the vacuum seal of
the wick assemblies noticed  during the second season of the project.

     6.   Methods to prevent piping episodes  in which macropores  and
micropores conduct  ponded  surface  water from either precipitation or
irrigation  into  the tray cavity area and  support  facilities  must be
perfected.  Solutions will  be dependent primarily on  limiting the amount of
ponding that occurs over  the  test plot.   Placement of tray lysimeters at
greater soil  depths would decrease the probability of  piping from macropores
since the  number and  frequency of flow events in  these  structures are thought
to decrease with depth (2).   From calamities experienced during the study

                                   86

-------
period,  it  has  been determined  that  it is more cost effective to prevent
piping events than to respond  to piping episodes  by providing sufficient  sump
pump capacity and capabilities to  handle highly variable  inflows of mud and
water.

Tube Lysimeters

     1.   The hammering  action used to drive the pipe section into the  soil
could have altered conditions  in- the  structure and  in the  position of the
encapsulated soils.  Any compression  of the  soil  material in the cores would
be expected  to have an adverse effect on the movement of  soil  water through
them.  The  tight soil conditions noted in the bottom of the lysimeters  were
not comparable to those observed in the bottom of the excavation from which
the encapsulated cores were removed.

     2.   The greater densities  of the soil observed in the tube lysimeters
could also affect the  amount  of water  caught.   It  is probable that,  when
water infiltrated the surface  soils above the tube lysimeters,  the tight  soil
surface  on  the  lysimeters created  a  perched water table in which the  free
water would  have flowed horizontally to the more  permeable zones that existed
in the backfill areas surrounding  the units.

     3.  Concentrated efforts must be made to adequately  compact backfill
soil  around tube lysimeter  installations.  In two instances settlement  of
fill material around tube  lysimeters,  caused by ponded conditions at the
surface, -led to  piping conditions that flooded  the  support facility via the
path of the  buried percolate collection lines.

     The  variability  in natural  soils also affected study  results.   The
differences in  soil properties  between test areas  and within test plots  in
addition  to  management of  activities  on the plots  affected  the percolate
flows that .were measured.   The field data recorded in each lysimeter resulted
from  the integrated influence of  all  local soil  properties on flow
conditions.  The variations in soils,  textures, densities,  stratigraphy,
chemical properties,  biological artifacts, and structure introduced
unexplainable differences  in response to hydraulic loadings.   Additionally,
difference  in soil  management above  the lysimeters during the project can
affect soil  properties  which  will  influence study results.   Since
tensiometers are the easiest means presently  available for measuring the
matric potential in soils,  their  utilization to control  the operation  of
individual  extraction lysimeters  will require their  emplacement in the soils
overlying the lysimeters.   Tensiometers, access ports to lysimeter support
facilities,  and additional  instrumentation devices located near the lysimeter
may clutter the  soil  surface and interfere with normal surface agricultural
operations  as they  are practiced elsewhere on the site.   This  factor,
combined with the  packing of the soil  caused  by  operators  servicing the
equipment in all  types of  weather,  can easily create  an  artificial  soil
environment  not representative of  field conditions.
                                   87

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                                REFERENCES

1.   Ayers, R. S.   Quality of Water  for  Irrigation.   In:   Proceedings
     Irrigation  Drainage Division,  Specialty Conference.   ASCE.  August 13-
     15,  Logan, Utah.  1975.  p.  24-56.

2.   Sevan,  K, and Peter Germann.   Macropores and Water Flow in  Soils.  Water
     Resources Research.  Vol.  18,  No.  2:   1311-1325.   October,  1982.

3.   Blackstock, D.  A.   Soil Survey  of  Lubbock County, Texas.   Soil
     Conservation Service, U.S.  Department  of Agriculture.   1979.  105 pp.

4.   Brown,  K. W., C. J.  Gerard, B. W. Hipp, and J. T. Ritchie.  A  Procedure
     for  Placing  Large Undisturbed  Monoliths  in  Lysimeters.   Soil  Science
     Society of America Proceedings.  Vol.  38:  981-983.   1974.

5.   Doorenbos,  J.,  and  W. 0.  Pruitt.  Guidelines for Predicting Crop Water
     Requirements.   Food and Agricultural Organization  Irrigation  and
     Drainage Paper 24.   Rome.   1977.

6.   Duke,  H.  R.,  and  H.  R.  Haise.  Vacuum  Extractors to Assess  Deep
     Percolation Losses  and Chemical  Constituents  of  Soil  Water:   Soil
     Science Society of America  Proceedings.  Vol. 37:   963-965.  1973.

7.  .Duke, H.  R., E. G.-Kruse, and G.  L. Hutchinson.   An Automatic Vacuum
     Lysimeter for Monitoring Percolation  Rates.   ARS 41-165  Agricultural
     Research Service,  U.S. Department of Agriculture.   Beltsville, MD.
     September, 1970.

8.   Hansen, V.  E.,  0.  W.  Israelson,  and G.  E. Stringham.    Irrigation
     Principles and  Practices.   4th Edition.  John  Wiley  and Sons,  New York,
     1980.   pg. 142.

9.   Jensen, M. E. (ed.).   Consumptive Use of Water  and  Irrigation Water
     Requirements.   American Society  of Civil Engineers.   ASCE Committee on
     Irrigation Water Requirements.   1973.

10.   Loehr, R. C.,  W.  J. Jewel, J. D.  Novak,  W. W.  Clarkson, and G.  S.
     Friedman.   Land Application of  Wastes, Vol.  2.   Van  Nostrand  Reinhold
     Environmental Engineering Series.   1979.  pg. 28.

11.   Matthess, G.  The Properties of Groundwater.   John Wiley and Sons.   New
     York.   1982.

12.   Mowery, I.  C.,  and  G. S.  McKee.   Soil Survey of  Lynn County, Texas.
     Soil  Conservation Service,  U.  S. Department of Agriculture.  1959.   37
     pp.

13.   Olson,  R. A., and L.  T. Kurtz.   Crop Nitrogen Requirements, Utilization,
     and   Fertilization.   In:  Nitrogen in Agricultural Lands.  F.  J.
     Stevenson, ed.   American Society of Agronomy Series on  Agronomy, No. 22.
     1982.   pg. 568.

-------
14.   Schoeller, H. (1956):  Geochimie des  eaux  souterraines.  Application aux
     eaux  de  gisements de petrole.   Rev.  Inst.  Petrol.  Ann.  Combust.  Liq.,
     10, Paris, pp. 181-213, 219-246, 507-552,  671-719, 823-874.  1955.

15.   Tanner,  C.  B.   Measurement  of Evapotranspiration.   In:  Irrigation of
     Agricultural Lands, R. M. Hagan, H. R. Haise,  and T.  W.  Edminston,  eds.
     American Society of Agronomy Series  on Agronomy, No. 11,  1967.   pg.  534-
 '   574.

16.   Texas Agricultural  Extension  Service.  Partners for Profit Coastal
     Sermudagrass, Fertilizer and Management.   B- 1223.  1979.

17.   Texas Department of Agriculture.   1983 Texas County  Statistics,   pg.
     171.

18.   U.  S. Environmental Protection Agency.  Process Design Manual  Land
     Treatment  of Municipal .Wastewater.   Center for Environmental  Research
     Information.  EPA 625/1-81-013.   October,  1981.

19.   Wendt, C. W.,  A.  B. Onken,  and 0.  C. Wilke.   Effects  of  Irrigation
     Methods  on Groundwater Pollutants  by Nitrate and  Other Solutes.   EPA
     600/2-76-291.  December, 1976.  pg.  6.
                                    89

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APPENDICES
    90

-------
      APPENDIX A
PROFILES OF TEST SOILS
         91

-------
                                 APPENDIX A

                       PROFILES  OF TEST SOILS (3, 12)


                            .  Amarlllo Series

Ap - 0 to 0.36 meters;  reddish brown  (SYR 5/4) fine sandy loam,  dark reddish
     brown  (5YR  3/4) moist; weak fine granular  structure; hard,  friable;  -few
     fine roots;  mildly alkaline; abrupt smooth  boundary.

B2H - 0.36 to 0.61 meters; reddish brown  (SYR 4/4)  sandy  clay loam, dark
     reddish brown  (SYR 3/4) moist weak coarse prismatic structure parting to
     weak  medium subangular blocky; very hard,  friable; common .roots;  many
     pores; thin  discontinuous clay  films  on prism  faces  and  patchy clay
     films on ped faces;  noncalcareous;  mildly  alkaline;  gradual wavy
     boundary.

B22t - 0.61 to 0.84 meters;  reddish brown (SYR 5/4) sandy clay loam, reddi'sh
     brown  (SYR  4/4)  moist; weak coarse prismatic  structure parting to weak
     medium subangular blocky; hard,  friable;  few roots; common pores;  nearly
     continuous clay films on prism faces and  patchy clay films on ped  faces;
     noncalcareous; moderately alkaline;  gradu-al  wavy  boundary..

B23t - 0.84 to 1.17 meters;  reddish brown (5YR 5/4) sandy clay loam, reddish
     brown  (SYR  4/4)  moist; weak coarse prismatic  structure parting to weak
     fine to medium subangular  blocky;  hard,  friable;  common pores;  few
     patchy clay  films  on ped faces;  few films  and  threads of calcium
     carbonate; calcareous; moderately alkaline;  gradual wavy boundary.

B24tca - 1.17 to  1.52 meters; pink (5YR 7/4) sandy clay loam,  reddish  yellow
     (SYR  6/6) moist;  weak coarse  prismatic structure parting to weak fine
     subangular blocky; hard, friable; many  soft  masses  and  weakly  cemented
     concretions  of calcium  carbonate, about 30  percent by volume;
     calcareous;  moderately alkaline;  diffuse wavy boundary.

B25tca - 1.52 to  2.03 meters; pink (SYR 7/4)  sandy clay  loam,  light reddish
     brown  (SYR  6/4)  moist; weak fine subangular blocky structure;  hard,
     friable; few  patchy  clay films;  many sand grains  bridged with clay
     films;, many soft  masses and weakly cemented concretions of calcium
     carbonate; calcareous; moderately alkaline.


                               Friona Series

Ap - 0 to 0.20 meters;  reddish brown  (SYR 4/3) sandy clay loam,  dark reddish
     brown (SYR 3/3) moist; weak fine  granular structure; slightly hard, vary
     friable;  many  fine roots; mildly  alkaline; abrupt smooth boundary.

B21t - 0.20  to 0.38  meters; reddish  brown  (SYR  4/3)  clay loam,  dark reddish
     brown (5YR 3/3) moist; moderate  coarse  prismatic structure parting to
     moderate  medium subangular blocky;  very  hard,  friable;  many pores; many

                                   92

-------
     worm casts; thin patchy clay films,  mostly on prism faces;  few  films and
     threads  of calcium carbonate  in  lower part;  calcareous;  moderately
     alkaline, clear smooth boundary.

B22t - 0.38 to 0.66 meters;  reddish brown (SYR  4/4) clay loam,  dark  reddish
     brown  (SYR 3/4) moist; weak coarse prismatic structure  parting to weak
     fine  subangular blocky;  hard, friable; many  fine pores,  common worm
     casts; thin patchy clay films, mostly on ped surfaces;  few  films,
     threads,  and  masses of calcium  carbonate;  calcareous;  moderately
     alkaline; abrupt smooth, boundary.

B23cam - 0.66 to 0.81 meters;  pinkish white (SYR  8/2) caliche;  indurated in
     the  upper part and  strongly  cemented in  the lower  part;  the upper
     surface  is laminar  and smooth; the lower part has pendants  of calcium
     carbonate as much as 1 centimeter long;  gradual wavy boundary.

B24ca - 0.81  to 1.52 meters;  pink  (7. SYR 8/4)  sandy clay loam,  pink (7.SYR
     7/4) moist; weak medium  subangular blocky  structure;  slightly hard,
     friable; about 50 percent  calcium carbonate  in  soft powdery  forms;
     calcareous; moderately alkaline.

-------
      APPENDIX  B



HYDRAULIC LOADING RATES
           94

-------
en
                                               TABLE B-1

                        HYDRAULIC LOADING JO BERMUDA GRASS AT THE GRAY SITE WITH
                          SOIL PERMEABILITY AT 4.39 CM/DAY (4% OF LOWEST RATE)

(1)
Month
January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
(crop)
(cm)
1.40*
2.16*
6.00
15.84
20.80
26.31
25.98
24.15
16.77
11.78
3.59*
1 . 50*
156.28
(3)
Pr
(cm)
1.96
2.95
4.11
4.76
10.11
10.85
9.53
9.27
10.44
8.76
2.74
2.60 '
78.08
(4)
Net ET
(2) - (3)
(cm)
-0.56
-0.79
1.89
11.08
10.69
15.46
16.45
14.88
6.33
3.02
0.85
-1.10
78.20
(5)
Percolation
(cm)


35.12
52.68
' 52.68
52.68
52.68
52.68
52.68
52.68
26.34

430.22
(6)
LW(P)
(4) + (5)
(cm)


37.01
63.76
63.37
68.14
69.13
67.56
59.01
55.70
27.19

510.87
      *Dormant vegetation

-------
vo
                                                TABLE  B-2

                      HYDRAULIC LOADING TO BERMUDA  GRASS SYSTEM AT  THE  HANCOCK SITE
                        WITH SOIL PERMEABILITY  AT 5.95 CM/DAY  (4% OF LOWEST RATE)

(1)
Month
January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
ET(crop)
(cm)
1.40*
2.16*
6.00
15.84
20.80
26.31
25.98
24.15
16.77
11.78
3.59*
1.50*
156.28
(3)
Pr .
(cm)
1.96
2.95
4.11
4.76
10.11
10.85
9.53
9.27
10.44
8.76
2.74
2.60
78.08
(4)
Net ET
(2) - (3)
(cm)
-0.56
-0.79
1.89
11.08
10.69
15.46
16.45
14.88
6.33
3.02
0.85
-1.10
78.20
' (5)
Percolation
(cm)


47.6
' 71.4
71.4
71.4
71.4
71.4
71.4
71.4
35.7

583. 1
(6)
LW(p)
(4) + (5)
(cm)


49.49
82.49
82.09
86.86
87.85
86.28
77.73
74.42
36.55

663.76
      *Dormant vegetation

-------
10
                                                TABLE B-3

                         HYDRAULIC LOADING TO COTTON AT THE GRAY SITE WITH SOIL
                             PERMEABILITY  AT  4.39  CM/DAY  (4% OF LOWEST RATE)

(1)
Month
January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
ET(crop)
(cm)
2.97*
3.97*
5.21*
6.50*
13.10**
11.57
24.03
29.00
19.96
11.07
3.46**
2.39*
133.23
(3)
Pr
(cm)
1.96
2.95
4.11
4.76
10. U
10.85
9.53
9.27
10.44
8.76
2.74
2.60
78.08
(4)
Net ET
(2) - (3)
(cm)
1.01
1.02
1.10
1.74
2.99
0.72
14.>50
19.73
9.52
2.31
0.72
-0.21
55.15
(5)
Percolation
(cm)



13.17

35.12
35.12
35.12
17.56



136.09
(6)
LW(P)
(4) + (5)
(cm)



14.91

35.84
49.62
54.85
27.08


•
182.3
       *Bare soil
      **Cover and bare soil in period

-------
                                         TABLE B-4

                  HYDRAULIC  LOADING  TO COTTON AT THE HANCOCK SITE WITH SOIL
                       PERMEABILITY  AT 5.95 CM/DAY (4% OF LOWEST RATE)

(1)
Month
January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
ET(crop)
(cm)
2.97*
3.97*
5.21*
6.50*
13.10**
11.57
24.03
29.00
19.96
11.07
3.46**
2.39*
133.23
(3)
Pr
(cm)
1.96
2.95
4.11
4.76
10.11
10.85
9.53
9.27
10.44
8.76
2.74
2.60
78.08
(4)
Net ET
(2) - (3)
(cm)
1.01
1.02
1.10
1.74
2.^99
0.72
14.50
19.73
9.52
2.31
0.72
-0.21
55.15
(5)
Percolation
(cm)



17.85

47.6
47.6
47.6
23.8
-


184.45
(6)
LW(p)
(4) + (5)
(cm)



19.59

48. 32
62.10
67.33
33.32
.


230.66
 *Bare soil
**Cover and bare soil in period

-------
<£>
<0
                                                TABLE B-5

                        HYDRAULIC LOADING TO GRAIN SORGHUM AT THE GRAY SITE WITH
                          SOIL PERMEABILITY AT 4.39 CM/DAY (4% OF LOWEST RATE)

(1)
Month
January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
ET(crop)
(cm)
2.97*
3.97*
5.21*
6.50*
10.92**
17.10
28.32
25.12
10.90**
6.83*
2.97*
2.39*
123.20
(3)
Pr
(cm)
1.96
2.95
4.11
4.76
10.11
10.85
9.53
9.27
10.44
8.76
2.74
2.60
78.08
(4)
Net ET
(2) - (3)
(cm)
1.01
1.02
1.10
1.74
0.81
6.25
18.79
15.85
0.46
-1.93
0.23
-0.21
; 45.12
(5)
Percolation
(cm)



13.17
17.56
35.12
35.12
35.12




136.63
(6)
LW(p)
(4) + (5)
(cm)



15.45
18.37
41.37
53.91
50.97




180.07
       *Bare soil
      **Cover and bare soil in period

-------
o
o
                                               TABLE  B-6

                       HYDRAULIC LOADING TO GRAIN  SORGHUM AT  THE  HANCOCK  SITE  WITH
                          SOIL  PERMEABILITY AT 4.39 CM/DAY (4% OF LOWEST RATE)

(1)
Month
January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
ET(crop)
(cm)
2.97*
3.97*
5.21*
6.50*
10.92**
17.10
28.32
25.12
10.90**
6.83*
2.97*
2.39*
123.20
(3)
Pr
(cm)
1.96
2.95
4.11
4.76
10.11
10.85
9.53
9.27
10.44
8.76
2.74
2.60
78.08
(4)
Net ET
(2) - (3)
(cm)
1.01
1.02
1.10
1.74
0.81
6.25
18.79
15.85
0.46
-1.93
0.23
-0,21
45.12
(5)
Percolation
(cm)



17.85
23.8
47.6
47.6
47.6




184.45
(6)
LW(p)
(4) + (5)
(cm)



19.59
24.61
53.85
53.85
66.39




227.89
       *Bare soil
      **Cover and bare soil in period

-------
   APPENDIX  C



NITROGEN LOADINGS
       10.1

-------
o
ro
                                                  TABLE  C-1

                      NITROGEN LOADINGS WITH 27 MG/L N WASTEWATER FOR THE GRAY SITE  AND
                       24 MG/L N WASTEWATER AT THE HANCOCK SITE  AND DESIGN LOADING FOR
                           TEST PLOTS USING EPA DESIGN CRITERIA FOR BERMUDA GRASS

(1)
Month


January
February
March
Apri 1
May
June
July
August
September
October
November
December
Totals
(2)
Pl-ET(crop)
(cm)

+ .56
+ .79
- 1.89
-11.08
-10.69
-15.46
-16.45
-14.88
- 6.33
- 3.02
- .85
+ 1.10
-78.2
(3)
U




(kg N/ha)



16.
52.
69.
87.
86.
80.
56.
39.
10.

500.



6
9
5
9
8
7
0
3
3

0
Gray


12.7
36.0
50.7
62.5
60.7
56.7
42.8
31.3
8.2

361.6
(4)
LW(N)
(cm)



Hancock


16.
45.
63.
78.
76.
71.
54.
39.
10.

455.


0
5
0
7
5
5
0
4
3

8



Gray


37.01
63.76
63.37
68.14
69.13
67.56
59.01
55.70
27.19

510.87
(5)*
LV)
(cm)



Hancock


49.
82.
82.
86.
87.
86.
77.
• 74.
36.

663.


49
49
09
86
85
28
73
42
55

76



Gray


13
36
55
55
55
55
43
32
8

352
(6)**
LV>
(cm)
Hancock


16
46
55
55
55
55
54
21
10

367
    *Column 5 is based upon three operational days per week.  These are project operational restrictions
     rather than what could be applied with the proper irrigation system.
   **Column 6 is what can be applied in three days per week from May to August.

-------
o
to
                                                  TABLE  C-2

                      NITROGEN LOADINGS WITH 27 MG/L N WASTEWATER FOR THE GRAY  SITE  AND
                         24 MG/L N WASTEWATER AT THE HANCOCK SITE AND DESIGN LOADING
                             FOR TEST PLOTS USING EPA DESIGN CRITERIA FOR COTTON

(1)
Month


January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
Pr~ET(crop)
(cm)

- 1.01
- 1.02
- 1.10
- 1.74
- 2.99
- .72
-14.50
-19.73
- 9.52
- 2.31
- .72
- .21
-55.15
(3)
U




(kg N/ha)






12.
24.
29.
20.
11.
1.

97.






0
0
0
0
0
0

0
Gray



10.0

9.7
8.2
8.0
9.0



44.9
(4)
LW(N)
(cm)



Hancock



6.

12.
10.
10.
11.



50.



0

3
3
1
4



1



Gray



14.91

35.84
49.62
54.85
27.08



182.3
(5)*
LW(p)
(cm)



Hancock



19.

48.
62.
67.
33.



230.



59

32
10
33
32



66

L

Gray



10.0

9.7
8.2
8.0
9.0



44.9
(6)**
LI
(D)
(cm)
Hancock



6.0

12.3
10.3
10.1
11.4



50.1
    *These loadings are based on two operational days per week at the cotton plots.

-------
                                             TABLE C-3

                 NITROGEN  LOADINGS  WITH 27 MG/L N WASTEWATER FOR THE GRAY SITE AND
                    24  MG/L  N  WASTEWATER AT THE HANCOCK SITE AND DESIGN LOADING
                     FOR TEST PLOTS USING EPA DESIGN CRITERIA FOR GRAIN SORGHUM

(1)
Month


January
February
March
April
May
June
July
August
September
October
November
December
Totals
(2)
Pr-ET(crop)
(cm)

- 1.01
- 1.02
- 1.10
- 1.74
- .81
- 6.25
-18.79
-15.85
- .46
1.93
- .23
.21
-45.12
(3)
U




(kg N/ha)





7.
28.
47.
41.
10.



135.





3
4
0
7
6



0
Gray



8.0
5.6
19.1
24.3
22.3




79.3
(4)
LW(N)
(cm)



Hancock



11.
7.
24.
30.
28.




101.



0
1
1
7
1




0



Gray



15.45
18.37
41.37
53.91
50.97




180.07
(5)*
LW(p)
(cm)



Hancock



19.
24.
53.
66.
63.




227.



59
61
85
39
45




89

L1

Gray



8
11
19
24
22




79
(6)**
W(D)
(cm)
Hancock



11

7
31
28




101
*These loadings are based on two operational  days per week at the grain sorghum plots.

-------
                  APPENDIX D



PERCOLATE QUALITY PARAMETERS"AT THE TEST PLOTS
                      105

-------
                                                                TABLE   0-1



                                 PERCOLATE   QUALITY   PARAMETERS   AT   TEST  PLOTS'
o
en
SOURCE
CRAY
TRAY 103
6a
so"
CVC
tc"
Ee
ky/haf
TRAY 104
G
SO
CV
1C
E
kg/ha
TRAY 105
G
SO
CV
XC
E
ky/ha
aG • geometric
bSD - standard
ALK CONO
i CaCO}/l) (


221. 8070.
47.4
21.2
50 100
2 1
135. 4923.







398.


too
1
71.6
mean
deviation
ITS pll TWI
«9/l) (ma N/l)


4652. 8.08 1.41
487. .184 .240
10.4 2.28 16.8
100
6 2 3
2838. 4.93 .862







3982.
770.
19.1
100

17-


CCV - coefficient of variation
NOg/NOj Nllj TOIAL P ODTIIO P ORG.P COO Cl 50^
(ng N/l) (og N/l) (ug P/l) (mg P/l) (ng/P) (pg/l) (iug/1) (wg/l)


1.56 .051 .29
.999 ' .097
50.5 91.9

7 7 1
.949 .031 .177







4.36 .026
4.31 .014
79.6 47.1
80 25
5 4
.784 .005
1C - percentage
*E • niaiber of


.025
.112
176.

6
.015







.017
.023
99.1

3
.003
of compos lie 'lafflple
quality determination


1665.
523.
29.8
88.9
9
1016.







50 1591.
245.
15.3
too
1 4
9 286.


80S-
88. 3
10.9
100
8
491.

530.



.'5.9

612.
40.2
6.56
too
5
110.
Ca
(ug/l)


280.
76.2
26.5
66.7
3
171.

560.



16.8

345.
60.8
17.5
100
2
62.2
£/!>


167.
39.6
23.2
66.7
3
102.

197.


100
5.9.

173.
6.36
3.67
100
2 .
31.2
K Ha TOC


35.9 1207.
2.65 }8.9
7.35 3.22
100 50
3 2
21.9 736.4

19



1
.57

24.'4 807.
3.54
14.4
100 100
2 1
4.39 145.
In total sampling effort
made for the
parameter
kg/ha- mass In kg/ha for material Intercepted by the unit

-------
                                                                 TABLE    0 -  I



                                                                      CONT.
SOURCE
GRAY
TRAY 106
Ga
su"
cvc
Le
kg/lu/
ALK
CaC03/l)







COND TDS pll TKN
(«g/l) (°x» N/l)







N02/N03
(«9 N/l)


40.2


,
2.41
Nil., TOTAL P
(09 N/l) (nig P/l)


2.29


1
.137
ORTIIO P ORG.P COD
(«9 P/D («9/P) (pg/D


.01


1
.001
Cl
(«9/D







S0<
("9/0







Ca
(oiy/l)







Mg







K
(og/l)







Na T(
(ng/l) («s







TRAY 104-106 DEPTH AVERAGE
G
SO
CV
XC
E
kg/ha
TRAY 107
G
SO
CV
XC
E
kg/ha
*G ' " geometric
bSD - standard
398


too
1
71.6

316.
12.0
3.80
too
2
104.
aic an
deviation
3982.
770.
19.1
100
3
717-

4426 3058. 7.48 .26
439.
14.3
too
1511
1461. 1009. 2.47 .086

6.31
14.7
131.
16.7
6
.568
,
37.5
11.3
28.6

7
12.4
"xc
.064
1.01
210.
20
5
.006

.0)6
.0)0
65.5

6
.012
• percentage of
.015 50.
.030 .
181.

4 1
.001 9

.015
.013
72.6

6
.005
1591.
245.
15.3
100
4
286.

108).
197.
18.0
too
to
357.
597.
49.3
8.63
83.3
6
53.7

488.
151.
30.2
100
II
161.
406.
130.
28.6
66.7
3
66.1

350.
139.
38.3
too
2
115-
181.
14.3
7.88
100
3
16.3

III.
59-4
49.9
100
2
36.7
22.4
4.40
19.4
66.7
3
2.02

10.3
2.40
23.3
50
2
3.40
807.


100
1
145.

424.


too
1
140.
conno* Ite *»«*>• In total sampling effort
e£ • number of quality determination Bade
for the
parameter
CCV • coefficient of variation
kg/ha- nass In kg/lia for natertat Intercepted by the unit

-------
                                                                        TABLE   D - I
o
oo




SOURCE ALK COND TDS pll TKN
(U9 CaCO}/l) («9/l) (ng N/l)
GRAY
TRAY 108
Ga
S0b
CVC
1C
Ea
kg/haf
TRAY 109
G
SO
CV
1C
E
kg/ha


213.
1.41
.664
100
2
87.3

418.


too
1
62.7
TRAY 107-109 DEPTH
G
SO
CV
1C
E
kg/ha
» geauetrl
286.
66.1
29.1
too
5
85.7
c mean


5467.
116.
2.12

2
2245.







AVERAGE
5162.
607.
11.9

3
1549.



3540. 7.85 .32
73.6 .028
2.08 .361
100
3 21
1451. 3-27 .131

2298.
187.
8.14
100
2
345.

3018. 7.73 .288
544. .214 .042
17.8 2.77 14.6
100
10 3 2
90S. 2.82 .087


CONT.
N02/N03 NII3 TOTAL P
(ug N/l) (ng N/l) (ng P/l)


57.6
37.1
57.7

7
23.6

10.8
4.49
39-0
16.7
5
1.63

30.0
30.9
77.7
95
19
9.01
"xc


.035
.374
184.

a
.014

.015
2.19
233.
14.3
7
.002

.057
1.28
318.
4.76
21
.017
• percentage of

ORTIIO P ORG.P
(og P/l) (ng/P)


.012
.Oil
77.2
.125
8
.005

.020
.017
69.7
too
5
.003

.015
.004
23.2
5.3
19
.004
conpotlu tanple

COD Cl
(pg/D («g/D


33. 1428.
438.
29.9
100 88.8
1 8
13.5 586.

549.
169.
29.7
too
3
82.5

33 1105.
4)0.
36.5
100 95.4
1 21
13.5 3)2.

S04 Ca


402. 3)4.
78.2 5.66
19.1 1.69
100 50
8 2
402. 137.

307. 38
43.9
14.1
100 100
6 i
46.1 5.7

402. 220.
13). 157.
31.8 54.5
too So
27 5
121. 66.1

Hg
(«g/D


iso.
13.4
8.92
SO
2
61.6

64.2


too
1
9.63

112.
46.6
38.6
80
5
33.7

if
(••u/U


14.
1.41
10. 1
50
2
5.74

16.



1
2.4

12.9
2.89
22.3
4o
5
3.88

Na TOC
(my/I) (ug/Q


616.
SI. 6
8.36
50
2
25).








544.
118.
21.3
66.7
3
163.
In total sampling effort
        SO « standard deviation
       CCV - coefficient of variation
eE    • number of  quality  determination made  for the parameter
 kg/ha* mass In kg/ha for  material  Intercepted by the  unit

-------













.
o
vo

SOURCE
(t
GRAY
TUBE IM
G*
so"
CVC
xcd
I*
kg/haf
TUBE 112
G
SO
CV
XC
E
kg/ha

ALK
ig Catty


689.
59-4
8.53
100
2
2,42.

507.
23-5
4.64
80
5
548.


COW) TOS
1) («9/D


3616.
321.
8.84

5
11244

4287.
749.
17-2

18
4630.


2269.
194.
8.54
100
a
7058.

2667.
365.
13.6
78.6
14
7058.

pll TKH
(ug N/l)


8.43 1.29
.148 1.62
1.75 92.7

4 5
26.2 3.89

7.62 .607
.264 .321
3.47 45.9
5.6
18 18
8.23 .656

N02/N03
(ng N/l)


4.06
5.62
74.2

20
12.6

196.
3.68
196.

10
212.
T
ta.3
(«g N/l)


.013
.017
102.9

19
.041

.053
,086
92.2

10
.057
ABLE 0-1
COHT.

TOTAL P OHTIIO P OAG.P
(ng P/l) («y P/l) (ng/P)


.019
.018
76.6

17
.058

3.36
1.25
35. 5

5
3/63


2.46
.90S
34.8
II. 1
9
7.66

.012
.008
61.2

IB
.013


.02



1
.062

.012
.012
88.4

II
.013

COD


26.9
7.64
27.9
SO
2
83.5

32.1
31.4
82.1

II
34.7

Cl


841.
165.
19.2
100
II
2617.

808.
240.
28.7
66.7
IB
872.

so4


157.
76.4
43.7
100
10
489.

525.
52.4
9.94
7.7
13
567.

Ca


119.
22.6
18.9
100
2
370.

230.
105.
36.6
too
9
249.

ha


72.1
8.98
12.4
100
2
224.

76.9
14.8
18.9
100
9
83.1

K
(wg/1)
•

27.9
7.78
27-3
100
2
B7.0

11.4
5.21
40.9
100
9
12.3

Ha
(«H»/D


947.
720.
63.9
100
8
2945.

528.


100
1
570.
TOC
dug/0


8.44
5.67
45.5

7
26.2







     TUBE 111-112 DEPTH AVERAGE
     G         553.      4131. 2515.
     SD        94.3      738.  369.
     CV        16.9      17.6  14.5
     1C      •  85.7            86.4
     E         7         23    22
     kg/ha
1162.
 G  » geometric mean
bSD • standard deviation
CCV - coefficient of variation
7.76 .710
.400 .865
5.15 93.4
4.5
22 23
16.3 1.49
1.72
5.69
too.

30
3.61
.021
.063
145.

29
.045
.060
1.59
195.

22
.127
.072
1.34
153-
3.7
27
.152
.012
.012
82.2

12
.025
31.3
29.0
79.4
7.7
13
65.6
820.
212.
25.1
79-3
29
1723.
327.
189.
50.6
47.8
23
687.
204.
113.
46.0
100
II
429.
76.0
13.8
17.8
100
II
160.
13.4
8.27
53.0
100
II
19.9
887.
703.
66.2
100
9
542.
8.4*
5.67
45.5

7
26.2
                                       XC   • percentage ofcomposite  sample In total sampling effort
                                      eE    • number of quality determination uade for the parameter
                                       kg/ha- uass In kg/ha for Material Intercepted by the unit

-------
TABLE   0-1
     COHT.
SOURCE AI.K
(ng CaCOj/l)
CRAY
TUBE' "3
G*
SLf-
CVC
xcd
te
kg/ha f
TUBE 1)4
G
SO
CV
1C
E
kg/ha


395.
91.0
22.6
100
4
399.

291.
108.
35.1
100
4
411.
COND HIS
(n9/0


2676. 159).
521. 188.
19.0 11.7
IS 100
20 10
2702. 1609.

3867. 2789.
715. 130.
18.1 4.66
7.1 100
14 II
5452. 3932.
pll TKN
' (ay N/l)


7.91 .443
.140 .271
1.77 52.3
33.3 28.6
6 7
7.99 .447

7.85 .588
.165 .305
2.10 46.6
28.6 28.6
7 7
11.1 .787
NtyNOj Nil, TOTAL P
(«9 N/l) (ng N/l) (uy P/l)


1.47
.989
56.8
10.7
28
1.49

.724
2.39
108.
9-52
21
1.02


.015 .033
.774 .079
264. 1)).
18.2
II 9
.015 .0)4

.026° .039
.06) .041
131. 81.9
16.7
12 6
.037 .054
OR] 110 P ORG.P COO Cl SOj Ca
(«9 P/l) (»g/P) (pg/l) («g/D (ay/I) («y/l)


.015 .01
.029
127.
8.3
12 1
.015 .010

.012 .07
.009
66.6
8.3
12 1
.017 .099


77.1 466.
12). 181.
100. 36.2
80 100
5 1)
77.8 471.

40.9 10)5.
3.0.2 50.5
64.6 4.88
75 100
4 I)
57.7 1459.


209. 90.3
42.2 41.8
19.9 42.8
100 100
1) 3
211. 91.2

45). 229.
52.6 92.6
11.5 38.)
100 100
12 )
6)9. )24.
Hg


33.6
.51)
15)
100
3
)).9

64.
9.76
IS.I
100
)
90.2
K
(»-J/D


D.I
6.25
44.6
100
3
13. i

20.5
15.6
100
)
28.9
Na TOC
(u'J/l) (uig/|)


)24. 11.9
2).) 29.7
7.08 77.2
100 100
2 2
)27. )2.2

609. 16.8
20.5 10.0
3.37 55.2
100 100
2 2
859- 2). 6
TUBE II3-H4 DEPTH AVERAGE
G
SO
CV
1C
E
kg/ha
*G " geometric
bSD - standard
339.
106.
29.7
100
8
411.
mean
deviation
3M4. 2136.
857. 627.
26.5 28.2
11.8 100
34 21
3767. 2585.


7.88 .491
.150 .286
1.91 48.8
30.8 28.6
13 14
9.53 .595


CCV - coefficient of variation
1.09
1.73
88.9
10.2
49
1.31
"xc
e£
fkg/lia
.036 .0)6
.5)8 .058
325. 107.
4
23 II
.044 .044
• percentage of
.01) .026
.022
120.
8.)
24 2
.016 .0)2
composite lample
- number of quality determination
- mass In kg/ha
58.2 695.
97.7 30).
110. 39.4
77.8 100
9 26
70.4 841.
303. 144.
1)2. 102.
40.2 59-9
100 100
25 6
687. 1/4.
146.
20.6
36.8
100
6
56.1
16.4
5.75
33.2
100
6
19.9
448. 21.5
16). 21.5
)4.6 76.1
100 100
4 4
542. 26.0
In total saaipllng effort
wade for the
parameter



for material Intercepted by the unit

-------
                                                           TABLE   D  -



SOURCE" ALK CONO TDS
(mg CaC03/l) (my/I)
GRAY
TUBE US
0
sub
cvc
1C
Ee
kg/ha f


296.
75.1
24.8
75
4
856.


3479- 2224.
489. 377.
13.9 16.7
8 85.7
25 14
10054 6427.

pit TKN
(ng N/l)


7.69 .641
.219 .411
2.85 58.9
20 28.6
10 7
22.2 1.85

N02/N03
(«0 N/l)


2.89
1.74
53.6
11.1
27
8.35

CONT.


NII3 TOTAL P ORTIIO P OR6.P COO
(ng N/l) (ng P/l) (nig P/l) (rng/P) (pg/l)


.049
.285
170.-
18.2
II
.144


.016
.025
no.

10
.046


.012
.014
96.4

12
.036


.01 26.7
43.4
107.
25 60
4 5
.029 77.1

Cl
(•19/1)


725.
64.5
8.88
78.6
14
2095.

S0«
(19/0


484.
61.8
12.5
83.3
12
1413.

Ca
(«3/0


232.
4.95
2.13
50
2
672.

Mil
(og/D


61.9
4.24
6.84
50
2
179.

K
(IKJ/D


15.5
.707
4.56
50
2
44.8

Na
(«9/D


563.
1.41
25.1
50
2
1627.

IOC
(«g/0


17.5
14.6
71-8
too
2
$0.6
TU
•
  BE
    cv
    *c
    £
    kg/na
               238.      3772. 2776. 7.72 .374
               3.54      596.  2771. .326 .374
               1.50      15.6  99.4  4.2276.9
               100       5.6   90    18.2 3) 3
               2         18    10    II
                                      3) 3
                                      9
10.5
6.09
53.9
15
20
26.3
.043
.142
152.2
25
12
.108
.01


16.7
6
.025
.014
.034
148.
9.1
II
.036
.01 33.6
68.6
109.
50
1 6
.025 84.4
924.
83.45
9.00
92.3
13
2318.
596.
48.8
8.16
91.7
12
1496.
299.
14.8
4.96
SO
2
751.
42.5
2.12
4.99
SO
2
107.
9.17
1.13
12.3
100
2
23.0
660.
63.6
9.61
50
2
1658.
15.5
.141
.912
100
2
38.9
  BE I I5-H6 DEPTH AVERAGE
c
CV
1C
kg/ha
275.
67.2
23.9
83.3

3599. 2439. 7-70 .474
551. 421. 27.3 .398
15.1 16.9 21.666.9
6.9 87.4 18.2 31.2
li a tit 11 •£
43 24 21 16
4.99
5.77
86.4
12.76
1.1
47
.046
.220
170.
21.7
23
.013
.021
114
6.25
.£
16
.013
.025
131.
4.3
23
.01
20
5
30.3
56.9
108.
55
II
81.8
814.
125.
16.2
85.2
27
540.
76.5
14.0
87-5
MI.
2«*
263.
39-3
14.9
50
712.
51.3
11.6
22.2
50
138.
11.9
3.72
30.1
75
32.2
610.
67.9
II. 1
50
1646.
16.5
8.86
49.5
100
44.5
SO
      getmetrlc wean
      standard deviation
CCV - coefficient of variation
                                                  dtC   •  percentage  of  compos life sample  In  total  sampling effort
                                                  6E     •  nunber of quality  determination made  for the parameter
                                                  fkg/lia*  nass  In  kg/ha  for  material  Intercepted by the unit

-------
ro
TABLE 0-1
COHT.
SOURCE AI.K
(ug CaC03/l)
GRAY
TRAY 201 .
Ga 228
sub
CVC
xcd too
Ee 1
kg/haf 280.
TRAY 202
G
SO
CV
xc
E
kg/ha
TRAY 203
G 154
SO
CV
JC 100
E 1
kg/ha 102.
aG <• geometric mean
bSO * standard deviation
CONO
(


4390
741.
16.7
12.5
8
5400.

5302.
247.
4.67
50
2
1909.

1358.
256.
18.6
33.3
3
897.


TDS
«9/D


3295.
165.
5.01
100
4
4052.

.344


100
1
1240.

1162.


100
1
767.


pll TKN


8.16 1.57
.205 .798
2.51 47.4
25 33.3
4 3
10.0 1.93

7.81 2
.233
2.99
50 100
2 1
2.81 .72

7.47 4.04
.431 1.12
5.78 27.3

3 2
4.93 2.67


N02/N03
(mg N/1)


22.3
29.9
57.0
9.0
11
27.5

13.1
17.1
67.6
25
4
4.71

3.99
17.3
95.5
8.3
12
2.63
"xc
eE
NH3 TOTAL P
(mg N/l) (og P/l)


.036 401
.102 .304
120. 66.8
16.7
6 2
.045 .493

.140 .01
.391
102.
33.3
3 1
.051 .004

.079
.181
98.8
9.1
11
.052
• percentage of
ORTIIO P
(«g P/l)


.062
.400
137.

8
.077

.057
.192
136.

3
.020

.212
.437
IIS.
7-7
13
.139
compos 1 to
ORG.P COO
(wg/P) (pg/D


41.1
8.04
19.3
66.7
3
50.5

50.


100
1
18.

50.


66.7
3
33.
Cl
(mg/l)


1063.
93.7
8.79
100
3
1307-








393.
33.1
8.39
too
3
260.
S04
(«g/»


633.
64.7
10.!
too
3
779.

524.


100
1
189.

171.
49.3
27.9
100
4
113.
Ca M0 K
(ng/l) («g/D (mg/l)


278. 113. 230.


100 100 100
1 1 1
342. 139. 283.








62. 25.2 24


too too too
1 1 1
40.9 16.6 15.8
Ha TOC
(ng/l) (rng/Q


17.5


too
1
21.5

18.8


100
1
6.77

23.4


too
1
15.4
sample In total sampling effort
- number of quality determination made
for the
parameter
        CCV ' coefficient of variation
                                                              f,
kg/ha* mass In kg/ha for material Intercepted by the unit

-------

SOURCE AlK COND TDS pll TKN
(119 CaC03/l) (ng/l) (ng N/l)
CRAY
TRAY 201-203 DEPTH AVERAGE
c* 187. 2027. 2790. 7.85 2.24
SD 52.3 1567. 895. .414 1.41
"^ 27.4 40.5 30.2 5.27 55.5
*c 100 23 100 22.2 100
E" f 2 13 6 9 6
Wh* 141. 1520. 2093. 5.89 1.68
TRAY 204
G
SD
CV
SC
E
kg/ha
\J1AY 206
SD
CV
SC
E
kg/ha
aG " geometric nean
bSD * standard deviation
TABLE
COHT.
N02/N0} NII3 TOTAL t
(ing M/l) («g M/l) (ng P/l)


9.59 .068 .117
27.9 .213 .335.
84.1 116. 109.
II. 1 19
27 20 3
7.20 .050 .088

.032
.052
94.5

^
.016
.01



1
.009
SC • percentage of
0 - 1
ORTIIO P ORG.P COD Cl 50^ Ca Hg
(u>9 P/l) (ug/P) (pg/l) (ug/l) (ug/1) (mg/l) (ug/l)


.119 45.9 647. 322. 131. 53.4
.397 6.47 373. 237.9 152.7 62.1
124. 13.9 51.1 60.7 W-9 89-9
4.2 71.4 100 100 100 100
24 76822
.089 34.5 485. 241. 98.5 40.0

.842
.107
12.6

2
.438
.05 1.02


100
1 1
.022 .439
composite sample In total sampling effort

K Na IOC
(uiij/.l) (nig/1) (1119/0


127. 19.7
146. 3-1
US. 15.6
100 100
2 3
95.3 14.8














e£ • number of quality determination made for the parameter
CCV • coefficient of variation
fkg/ha- mass In kg/lia for material Intercepted by the unit

-------
                                                               T A B I E

                                                                    CONT.
                                                                            D  -  I
SOURCE ALk COND TOS pll TICK
(og CaCOj/l) (iug/1) (nig N/l)
GRAY
TRAY 20d-206 DEPTH AVERAGE
a4
sob
cvc
£e
kg/haf
TRAY 207
G 8.11
so
CV
tc
E |
TRAY 208
G
SO
CV
tc
e
kg/ha
N02/N0j .Nil,
(«H) N/l) (ug N/l)
.025
.052
112.
5
.009
.226 .01
1.59
Idt.
2 1
.065 .003
.01 .39
.0002 .008
TOTAL P ORTIIO P ORG.P COD Cl SO^ Ca Hg K
(ng P/l) (my P/l) (utg/P) (pg/l) (»!l/l) (rag/1) (wg/ll (uig/l) (mg/
.106 1.02
80.2
100
3 1
.036 .d39
.Od9
.Old
2
.Old
.98
1
.020
*6  * geometric iiean
bSD - standard deviation
CCV * coefficient of variation
 tC   • percentage of cooiposlta sample In total sampling effort
eE    • number of quality deteiwlnatlon Bade for the parameter
 kg/haa mass In kg/ha for Material Intercepted by the unit

-------

SOURCE

AI.K
1 CaC03/l)


COHD 70S
(«J/D
GRAY
TRAY 207-208 DEPTH AVERAGE
G*
so"
cvc
Ee
kg/haf
TUBE 211
G
su
CV
tc
E
kg/ha
TUBE 212
C
SO
CV
SC
E
kg/ha
aG » geometric
bSO • standard

169.
14.8
8.76
100
2
98.1

195.
25.2
12.9
75

130
mean
deviation

6161.
719.
11.6
8.3
12
3573.

4170.
389.
9.29
15.4
13
2794.

5098.
460.
8.98
too
8
2957.

2936.
41.3
1.41
100
3
1967.
T A B L E 0 - 1
COHT.
pll TKN
(ng N/l)
8.11
1
2.35

7.93 1.33
.106 1.02
1.34 66.4
50 33.3
2 3
4.60 .769
*
7.98 .305
.49 .587
6.13 114.
66.7 100
3 2
5.35 .204
N02/N0}
(•9 N/l)
.080
2.93
172.
3
.014

16.5
25.8
46.0
5.3
19
5.32

80.8
38.9
39.8
14.3
14
.040
Nl!3
(«9 N/l)
.063
.269
•34.
2
. .Oil
.\

.070
.068
70.7
12.5
8
.041

.060
.108
112.
66.7
3
.040
TOTAL P ORTIIO P OflG.P COO
(»g P/l) (mg P/l) to/P) (pg/1)


.014
.007
47.3
50
2
.008







1C • percentage



eE
» number of
.014
.537
149.
3
.002

.022
.050
129.
8.3
12
.013

.016
.053
167.
33.3
6
.010
of composite sample
quality determination


48.6
2.31
4.74
66.7
3
28.2

79-9
178.
126.

3
53.5
Cl S04 Ca Mg K Na TOC
(•9/1) (^/l) (»9/l) (n9/U (uxj/l) (mg/1) (ng/Q


2142. 522. 564. 92.6 13.0
230.6 263.
10.7 40.4
100 100 100 100 100
6 a i i i
1242. 303. 327. 53.7 7.54

806. 416.
59.8
14.2
100 66.7
3
540. 279.


31.6


too
1
19.5

8.88
2.48
27-3
100
2
5.95
In total sampling effort
.Bade
for the parameter

CCV * coefficient of variation
kg/ha- nass In kg/ha for material Intercepted by the unit

-------

SOURCE
CRAY

AI.K
(109 caoyi)


COND


TDS pll
(09/1) («


TKH
•9 N/l)


N02/N03
("9 N/l)

TABLE
com.
HI,
<«J N/l)

TOTAL P
<«9 P/l)

0 - 1

ORTIIO P OAG.P COO
(ng P/l) («g/P) (pg/l)



Cl
<«9/l)


S°<


Ca
(«a/i)


M9
(ug/U


K Na TOC
(»9/l) («g/D («9/0

TUBE 2 11-2 12 DEPTH AVERAGE
G*
sub
CVC
xc
Ee
kg/haf
185.
24.7
13.2
83.3
6
117.
5029.
1166.
22.6
12
25
3169.
4396. 7.96
1088. .352
24.1 4.42
100 60
II 5
2763. 5.01
.737
.959
85.0
60
5
.464
32.3
37.8
51.3
9.1
33
5.32
.067
.075
27.3
77.4
II
.044
.014
.007
47.3
50
2
.008
.019
.049
136.
16.7
IB
.012
62.3
123.
130.
83.3
6
39.3
1863.
551.
28.1
100
7
1173.
491.
246.
42.0
90.9
II
309.
564.


100
1
327.
92.6


100
1
53.7
13.0 13.8
14.3
82.9
100 100
1 3
7.54 8.72
TUBE 2 13
G
SO
CV
tc
E
kg/ha
TRAY 301
G
SO
CV
1C
E
kg/ha
196


100
1
7.84

208.
7-78
3.73
too
2
358.
5338.
212.
3.97
50
2
214.

2780.
142.
5.10
25
8
4781.
2376. 7.84


100 100
1 1
2957- 4.60

1796. 7.46
188. .456
10.4 6.11
100 40
7 5
4052. 12.8







.462
.248
48.3

3
.795
15



1
5.32

5.73
6.70
58.9
8.3
12
9.85







.044
1.36
270.
II. 1
9
.076







.049
.049
56.9

3
.085
.01



1
.0004

.014
.064
196.

8
.025







.10 37.1
15.8
40.8
50
1 2
.172 63.9







677.
102.
14.9
100
8
1164.







255.
96.7
35.6
100
9
438.







132.
16.3
12.3
too
2
227.







52.9
4.31
8.15
too
2
90.9







18.9 268. 26.1
1.41
7.44
100 100 100
2 1 1
32.6 461. 45.8
*G  * geometric mean
bSD - standard deviation
CCV - coefficient of variation
• percentage of composite  sample  In  total  sampling effort
• number of quality determination Bade  for the parameter
  mass In kg/ha for Mterlal  Intercepted by the unit

-------


SOUHCt
CRAY
TRAY 302
Lb
cvc
tc
kg/l.af


ALK
(•ig CaCiyi)

208.
84.2
38.6
75
691.


CUNO

2254.
1336.
52.8
71
14
7484.


TDS pll TKN
(aig/l) («9 N/l)

1628. 7.60 .798
1336. .366 1.21
52.8 4.81 96.6
64.3 II. 1 It.l
14 9 9
5404. 25.2 2.65


N02/M03
(«>9 N/l)

4.71
8.49
64.8
3.7
27
15.6
T A

NH3
(«9 N/l)

.090
.772
239.
5.3
19
.299
B L E
COMT.
TOTAL P
(«9 P/D

.071
.077
70.0

4
.237
D - 1

ORTHO P
(ma P/l)

.051
.718
223.
4.8
21
.169




ORG.P COO Cl
(«9/P) (P9/D (uig/l)

•01 35.0
9.67
26.9
40
2 5
.033 116.

769.
93.7
12.1
100
10
2554.


so4
<«>9/l)

264.
80.0
28.8
90.1
II
878.


Ca
<*>!)/ 1)

232.
62.4
26.1
100
3
773-


Hg
(nig/l)

93.8
21.8
22.8
100
3
311.


K

35.9
5.64
15.6
100
3
119.


Na
(ug/l)

497.
266.
50.2
too
2
1650.


TOC
(eig/0

20.5
5-78
27.7
50
2
68.0
TRAY 303
G
SO
CV
SC
E
kg/ha

965. 707. 8.52 .257
410. 233. .050 .396
40.4 31.7 58.1 104.
25 100 50
4422
1496. 1095. 13.2 .398

2.57
4.11
99.9
12.5
8
3.99

.028
.058
107.
14.3
7
.043

1.6



1
2.48

.417
.627
95.2

7
.646

.01



1 .
.016

21.2
13.7
58.9
50
2
32.8

130.
52.9
37.4
100
6
202.

69.8
43.4
53.4
too
7
108.

39.


100
1
60.5

19.6


100
1
30.4

20.


100
1
31.

15.9


100
1
24.6
G
CV
1C
208.
65.5
30.5
83.3
2110. 1464. 7-67 .603
1147. 1169. .497 1.04
48.3 57.3 6.48 107.
15.4 80 25 7.1
26 25 16 14
4685. 3250. 17.0 1.34
4.47
8.06
72.4
6.4
47
9.92
.059
.895
284.
8.6
35
.132
.106
.534
186.
8
.236
.058
.636
197.
2.8
36
.129
.018
.045
139.
4
.039
31.7
11.8
34.8
44.4
9
70.4
473.
279.
47.6
100
24
1050.
185.
115.
512.
96.3
27
410.
143.
91.9
54.0
100
6
318.
59.7
34.8
50.6
100
6
132.
26.3
9.95
35.8
100
6
58.5
434.
242.
54.6
too
3
965.
20.5
5.51
26.1
75
45.6
 G  • geometric mean
bSl) - standard deviation
CCV • coefficient of variation
'kg/ha-
percentage of composite sample In total sampling effort
number of quality determination uade for the parameter
mass In kg/ha for material Intercepted ty the unit

-------
00

SOURCE AI.K
(tig CaC03/l)
GRAY
TRAY 304
6a
sob
CVC
xcd
Ee
kg/haf
TRAY 305
G
SD
CV
1C
E
kg/ha

COND TDS pll TKN
(ng/U (ug N/l)


4090. 2082. 8.21
20.5
.984
too
1 2 1
695. 35*. 1.40 '

15*5.
49.5
3.2
50
2
1121.

N02/M03
(ng N/l)


3.80
.361
9.48

2
.645

.491
2.06
68.8

3
.353
TABLE
CONT.
Nllj TOTAL P
(ng N/l) (tig P/l)


.043
.107
125.

It
.007

.091
.150
110.

3
.066
D - 1
TTRTliO P
i«3 P/D


.127

35.5

4
.022

.01



3
.007

ORG.P COO
(og/P) (pg/l)


50.8


100
1
8.64

49.7 17.9



1 |
35.8 12.9

Cl
(«9/l)


779-
93.8
11.9
100
3
1.36.

629.
32.5
5.17
50
2
453.

so4
H/D


359.
48. 1
13.3
75
*
61.0

149.
55.2
J5.8
50
2
107.

Ca
(my/I)


107.


too
i
18.2

120.



1
86.4

Hg K Na TOC
(mg/l) («y/l) («g/l) (uy/Q


26.


100
1
4.42

22.



1
15.8
TRAY 304-305 DEPTH AVERAGE
G •
SD
CV
XC
E
kg/ha
* geometric iiean
* standard deviation
4090. 1793. 8.21
312.
17.2
75
1 4 1
695. 807. 1.40


l.ll
1.68
57.6

5
.500
"xc
e£
.059
.118
110.

7
.027
• percentage of
.043
.075
92.5

7
.019
50.2 17.9
.778
1.55
50
2 1
22.6 12.9
715.
107.
14.8
BO
5
352.
266.
116.
39.7
66.7
6
120.
113.
9.19
6.10
50
2
50.9
23.9
2.83
11.8
50
2
10.8
conpoilt* sample In total sampling effort
• number of quality determination made
for the
paraueter
        "SO
        CCV • coefficient of variation
ky/ha* mass In kg/lia for material Intercepted by the unit

-------
                                                                 TABLE     0 -

                                                                      CONT.
SOURCE ALK
(ng CaCOj/l)
GRAY
TRAY 307
C 212
sob
cvc
tt"
E6 I
kg/haf 27.6
TRAY 308
G 270
SO
CV
1C
E 1
k9/l« 27.
TRAY 309
SO
CV
SC
E
kg/ha
COND IDS pll TKH
(ng/1) (ug N/l)


IOJ8. 8.17 1.18
84.9
8.01

2 1 1
138. 1.06 .153

540 8.71


100 100
1 1
54. .871
1522. 8.08 1.08
86).
52.7

2 1 1
654. 3.47 .46*
h02/N03 NII3 TOTAL P OKTIIO f ORG.P
(09 N/l) (ng N/l) (ng P/l) (109 P/l) (ng/P)


.983 .20 .03 .01 .01
4.16
134.

2 till
.128 .026 .004 .001 .001

.17

i

1
.017
.394 .028 .10
1.26 .050
100. 110.

3 2 1
.169 .012 .043
COO C1 S04 Cs Mg K Na TOC
(pg/1) (»g/l) (og/l) («g/l) («g/l) (ng/l) (09/1) (og/i


5.4.9 132. 14).
11.3
7.91
50
112
7.14 17.2 18.6

135.


100
1
13.5
169. 64. 18. 4.0 IS.



1 1 1 1 1
72.7 27.5 7-74 1.72 6.45
aG  - geometric nean                                 dSC   • percentage of  compos Itesoivle 
-------
                                                                      TABLE
                                                                                     - I
                                                                           COHT.
ro
O
SOURCE ALK COND
(»j CaC03/l) (
GRAY

TRAY 307-309 DEPTH
G«
SDb
CVC
1C
I*
kg/haf
rE 311

SO
CV
xc
E
kg/ha
TUBE 312
G
SO
CV
1C
E
kg/ha
239.
*I.O
17.0
SO
2
52.6

153.
62.9
39.0
66.7
3
76.6

**8.
8*.9
18.8
100
2
8*2.-:

AVERAGE
1070.
635.
53.5
20
5
235.

3246.
1718.
49.1
33.3
3
1623.

3029.
871.
27.6

9
569*.
TOS
m/1)









3*10.
3*2.
9.99
33.3
3
1705.

2188.
118.
5.39
100
9
*M3.
pll TKN
(ng N/l)


8.32 1.13
.3*0 .071
*.09 6.26
33.3
3 2
1.83 .2*8

8.09 .*63
.021 .83*
.262 III.
SO SO
2 2
4.04 .232

7.92 .*9*
.3** .297
4.34 51.6

7 8
14.9 .928
R0.,/N03
(ng N/l)


.465
2.3*
.465

6
.102

12.3
20.5
9.7-9
25
*
6.13

7-38
22.*
108.

IS
13.9
NII3
(ng N/l)


.05*
.096
99.5

3
.012

.077
.263
131.
33.3
3
.038

.035
.1**
IS).

IS
.065
TOTAL P ORTIIO P ORG.P
(ng P/l) (mg P/l) d>g/P)


.03



1
.00*

.02*
.032
96.*
66.7
3
.012

.017
.012
57.7

7
.033


.252
.086
1**.

3
.OSS

.018
.05
1*3.
25
*
.009

.018
.072
IBS.

13
.033


.01



1
.001

.032
.021
60.6
50
2
.016

.01

'

1
.019
COD
(P9/D


96.3
80.7
72.1

2
21.2

26.1
16.3
57.1
so
2
13.0

12.*
33.2
125.

2
23.*
ci so4
(ng/l) (ng/l)


132.



1
17.2

13720.
2.83
.206

2
6860.

671.
96.*
14.2
too
to
1261.


IIS.
38.9
32.1
75
4
25.3

696.


100
1
3*8.

369.
56.*
15.1
100
9
69*.
Ca Hg K Na TOC
(•(I/O (wg/D (ng/D («g/l) dm/I)


18. *. is.



i i i
7.7* 1.72 6.*5

5*3. 12.2
33.3
6.11
100 100
2 1
271. 6.1

1*1. 56.8 20.9
55.7 *.78 2
37-6 8.3* 9-5
100 100 100
3 3 3
265. 107. 39.*
       C  - geometric mean
      bSO > standard deviation
      CCV - coefficient of variation
 1C   • percentage  of  conpoilte sample  In total sampling effort
8£    • number of quality determination made for  the parameter
'kg/ha- nass In kg/ha  for Material  Intercepted by the unit

-------
TABLE    D - I



     COHT.
SOURCE ALK
(«g CaC03/l)
GRAY

CONU TOS

pll TKN
(ng N/l)

N02/N0j NII3 TOTAL P OHTHO P ORG.P COD Cl SO^
(ag N/l) (ng N/l) (og P/l) (wg f/l) (og/P) (pg/l) (ng/l) (ny/l)



Ca

Mg
(«g/D

K

Na
(«g/D

TOC

TUBE 311-312 DEPTH AVERAGE
C
sub
cvc
xcd
Ee
f
kg/ha'
JJJBE 313
SD
CV
XC
E
kg/ha
TJJBE3I4
SD
CV
XC
E
ky/ha
BU " geometric
bSO * standard
235.
171.
6158.
80
5
280.
279.
61.7
21.8
66.7
3
474.
286.
32.0
ll.l
too
6
948.
mean
deviation
3082. 2445.
1113. 584.
34.4 23.4
8.3 9.2
12 12
3667. 2909.
3869. 2780.
679. 741.
17.3 25.9
18.8 100
16 4
6578. 4726.
4041. 3104.
1170. 694.
27.9 21.9
15 100
20 II
11374.10276


7.96 .488
.306 .389
3.85 63.7
ll.l 10
9 10
9.47 .580
7.97 .452
.272 .467
3.42 83.4
66.7 100
3 2
13-5 .769
7.65 .464
.353 .498
4.61 76.5
20 26.6
10 7
.25.3 1.54


CCV « coefficient of variation
8.21
21.4
104.
5.3
19
9.77
.156
74.7
239.
IB.B
16
2.65
10.0
21.6
109.
4.5
22
33.2
d*c
e£
fkg/h*
.940 .019
.163 .019
145. 79-1
5.5 10
IB 10
.047 .023
.179 .017
.203 .014
85.6 70.7
50
4 2
.304 .029
.029 .014
.069 .034
121. 149.
7.7
13 7
.096 .046
.018 .022 18.0 756. 393.
.066 .016 21.4 2.84 114.
176. 60.5 77.6 .036 28.1
5.9 33.3 25 83.3 100
17 3 4 12 10
.021 .026 21.4 899. 468.
.016 .017 49.5 819. 417.
.076 .0)4 49.5 163- 359.
202. 70.7 99-7 19.7 69.2
II. I 100 100 100
9 2324
.027 -029 84.2 1392. 708.
.106 .01 41.9 955. 657.
.114 45.4 387. 176.
244. 86.0 38.3 26.2
6.7 20 100 100
15 4 5 12 12
.055 .033 137. 3)62. 2175.
141.
55.7
37;6
100
3
265.






459.
222.
43.9
100
5
1519.
S6.8
4.75
8.34
100
3
107.






80.9
22.6
26.9
100
5
268.
20.9
2.
9.5
100
3
39.4






7.92
3.65
41.6
100
5
26.2
543.
33.23
6.11
100 .
2
271.






511.
256.
44.3
100
4
1690.
12.2


100
1
6.1
13.2
9.40
63. B
100
2
22.4
6.3


100
1
20.9
• percentage ofcompotlte sample In total sampling effort •
- number of
quality deteiulnatlon made fur the parameter
* nass In kg/ha for material Intercepted by the unit

-------
                                                                      TABLE
                                                                                   D  -  I
f\>
ro

SOURCE ALK CONO TDS pit TKN N02/N0j
(ng CaCOj/l) (ng/D (»9 N/l) (ng N/l) {
GRAY
TUBE 313-314 DEPTH AVERAGES
6* 284. 3964. 3014. 7.72 .462 4. SB
SUb 40.0 978. 695. .352 .438 49.8
CVC 13.9 24.0 22.5 4.55 73-5 190.
XCd B8.9 16.7 100 30.8 44.4 10.5
Ee 9 36 IS 13 9 38
' kg/haf 713- 9949. 7566. 19.4 1.16 II. $
G
SO
CV
XC
E
kg/ha
G
SO
CV
XC
E
kg/ha
aG - geometric wean XC
bSD • standard deviation eE
com.
WI3 TOTAL P ORTIIO P ORG.P COD Cl S04 Ca Mg K Ha TOC
[ug N/l) (mg P/l) (ng P/l) («g/P) (pg/l) (ng/l) (ug/l) (ay/I) («g/l) (ug/l) (my/1) (uig/0
.044 .015 .016 .012 39.0 935. 586. 459. 80.9 7.92 511. 10.3
.132 .030 .099 .028 43-4 165. 233. 222. 22.6 3.65 256. 8.25
133. 135. 230. 210. 84.0 16.8 36.4 43.9 27.0 41.6 44.3 69.1
17.6 8.3 50 100 100 100 100 100 100 100
17 9 24 5 6 14 16 5 5 5 4 3
.III .037 .041 .030 97.9 2346. 1472. 1519. 268. 26.2 1690. 25.8
- percentage ofcompo,|te sample In total sampling effort
* number of quality deteralnatlon nade for the parameter
        CCV • coefficient  of variation
kg/ha* nass In kg/ha for uatertal Intercepted by the unit

-------
ro
CO

SOURCE AI.K
(nj CaCOj/l)
HANCOCK.
TRAY 101
G1
so"
cvc
it" -
te
kg/haf
TRAY 102
G 238.
SI)
CV
tC too
E |
kg/ha 390.
TRAY 103
G 100.
SO
CV
1C
E 1
kg/ha %7 5
aG - geooietrtc mean
bSO = standard deviation

CONO
1


4)50.
813.
19.6

2
2117.

3570.
1089.
29.3
71.4
7
4355.

5470.
70.
1.28
too
2
2407.



TDS
[»3/l )


2429.
510.
20.7
100
3
1239.

2831.
428.
15.0
75
4
3454.

3436.


100
1
1512.



pll TKH
to H/l)


7.79 .15
.141 .099
1.81 66.

2 2
3.97 .077

7.28 .490
.427 .287
5.87 48.4

3 6
8.88 .598

.692
.131
18.7

3
5.39 .314


CCV • coefficient of variation

T A 6 I E
CONT.
N02/N03 Kllj TOTAL P
to N/l) (my N/l) (eg P/1)


18.3
16.4
72.6

4
9.35

1.52
9.85
162.

10
1.85

.84
5.02
177.

8
.369
d*C
«£
fkg/ha


.066 .03
.067
79:6

5 I
.034 .015

.053 .021
i 136 .024
137. 85.8

II 4
.065 .025

.02



1
.009
• percentage of
0 - 1

ORTIIO P OKG.P COO
(ug P/1) (mg/P) (pg/1)


.031
.173
157.

3
.016

.014
.025
123.

6
.017

.01



k
.00k
conipo* Ite sample
• number of quality determination
- nass In kg/ha


102.
124.
85.4

^
51.8

61.8
35.7
49.8

4
75.4

36.9
15.2
38.9

3
16.2



Cl SOj Ca Hy K Ha
(119/1) (og/1) (oig/l) («g/l) (oig/1) (ng/l)


917.
152.
16.3
100
4
468.

1121.
268.
23.3
75
8
1368.

1555.
435.
27.2
33.3
3
684.


179.
77.3
1,0.8
100
6
91.2

181.
59.6
31.4
100
7
222.

227.
21.7
9.55
33.3
3
99.8


539. 378. 26.
2.10

100 100 100
1 1 1
275. 193. »3.3

375. 91.4 16.4 22.
90. 9.
23.5 2.30 50.
66.7 66.7 66.7 100
3331
457. III. 19.9 26.8







TOC
(uig/Q









14.9
t.88
32.

2
8.45

9.28
2.12
22.6

2
4.08
In total sampling effort '
made
for the
parameter
for naterlal Intercepted by the unit

-------
r\>
•£»

SOURCE ALK CONO TDS pit TKN
(ng CaCOj/1) (ng/l) (ng N/l)
HANCOCK
T«AY 101-103 DEPTH AVERAGE
c 160. 3959. 2738. 7.d8 .d37
50 91.9 1120. $08. .dl8 .287
CVd 53.1 27.2 18.3 5.58 52.6
*£ 50 dS.S 75
E f 2 II 8 5 II
k9/li» 115. 2850. 1971. 5.39 .)ld
TRAY lOd
G
SO
CV
1C
E
kg/ha
TRAY 105
G J7dd.
SO
CV
1C 100
E 1
kg/ha 2d7.
aC o geometric Bean
LSO • standard deviation

TABLE
CONT
D - 1

NtyHOj Wlj TOTAL P ORTIIO P ORG.P COO Cl SO^
("9 N/l) («g N/l) (ng P/l) (wj P/l) (og/P) (pg/l) (ug/1) (u.g/1)


1.92
ld.3
181.

22
1.38

68. d


100
1
6.15

123.



1
Id. 8
d»C
«E


.057 .022
.116 .019
122. 69.0

16 6
.Odl .0)6

.15


too
1
.Old

.Id



1
.017
- percentage
• number of


.015 '6d.d 1135.
.08d . 85.3 352.
221. 95. d 29.8
73.3
13 H IS
.Oil d6.3 817.

SO


too
1
d.5

.01 502.3
20.5
d.oB
100
1 2
.001 60.3


188.
£0.9
31.0
87.5
16
135.








333.
d3.6
13.1
too
2
39.9

Ca


dio.
107.
25.2
75
d
295.








2Sd.



1
30.5

Hg K Na IOC


130. 18. d 22. 11.7
I.d3 35.7 d.S7
.879 179. 37.0
75 75 100
d d 1 d
93.8 13.2 26.8 8.1.5








177. 26.


100 100
1 1
21.2 3.12
of composite' *M>pl« In total sampling effort
quality doternlnatlon made for tlia
parameter
        CCV • coefficient of variation
kg/ha* nass In kg/ha for naterlal Intercepted by the unit

-------
                                                                       TABLE
                                                                                    D - I
                                                                            CONT.
IVJ
cn
SOURCE ALK
(mg CaCOj/1)
HANCOCK
CONO TDS pit TKN
(n>9/l) (mg N/l)

N02/N03
(«9 N/l)

HII, TOTAL P onTHo P ORG.P
(mg N/l) (mg P/l) (ug P/l) (mg/P) (

COO
P9/I)

Ct

S04 Ca Hj K Na
[i"J/D («"J/0 (ni'j/1) (my/I) (my/I)

TOC
<»g/1

TRAY 104-105 DEPTH AVERAGE
G4
sob
CVC
V*
Ee
kg/haf
TRAY 108
& 128.
SO
cv
1C
E l
kg/ha 52.5
TRAY 109
G
SO
CV
«C
E
kg/ha
*G « geometric mean
bSO • standard deviation
2744.


100
1
247.

6866. 5193. 7.91 .759
806. 748. .014 1.57
11.7 14.3 .178 102.
75
2424
2815. 2129. 3.24 .3H

1.29



1



91.8
38.9
40.6
50
2
10. 1

184.
229.
60.2

a
75.5

446.



1

d»C
eE
.145 .01
.007
4.90
50
2 1
.016 .001

.085 .028 .01
.131 .049
87.9 109.

72 5
.035 .Oil .004

.10 .23



1 1

- percentage of compos 1 to sample
• number of quality determination
50.


too
I
4.5

103.
99.3
75.1

4
42.1

1)4.



1

502.
20.5
4.08
100
2
60.3

679.
341.
45.5
20
5
278.

1420.



1

333. 254. 177. .26
43.8
13.1
100 100 100
2111
39.9 30.5 21.24 3.12

232. 627. 266. 30.
30.0
12.8
. 100 100 100
5 II 1
95.2 257. 109. 12.3














47.



1
19.

17-



1

In total sampling effort
made
for the
parameter

       CCV - coefficient of variation
kg/h«" mass In kg/ha for material Intercepted by tliu unit

-------
ro

SOURCE ALK
(ng CaC03/l)
HANCOCK

CUNO


TDS pii TKN
(»»J/l) (ng N/l)


N02/H03
(ng N/l) 1

TABLE
CONT.
NII3 TOTAL P
[ng N/l) (og P/l)

D - 1
ORTIIO P
(ng P/l)


££i


COO Cl
i (pg/D («g/D


SO^ Ca
(wg/1) (iug/1)


Kg
(my/I)


K
(119/1)


Na TOC
(>*j/l) (ug/Q

TRAY 108-109 DEPTH AVERAGE
G* 128.
sub
CVC
JC
E* 1
kg/ha 52 5
TUBE 113
351
?!J 89- »
cy 2d.e
« 62.5
t /h 8
kg/ha Jm.
TUBE lid
6 299.
SD 20.9
" 6.99
JC ,00
E i,
kg/ha ,288.
*G » geometric mean
SD * standard deviation
6866.
806.
11.7

2
28)5.

20 7d.
270.3
12.9
7.7
39
5193. 7-91 -8dd
7d8. .Old 1.37
Id.) .178 91. d
75
d 2 5
2129. 3.2d .187

Id6l. 7-51 .277
76.9 .395 .d55
5.26 5.26 108.
82.) 15
17 22 20
22dl6 15790 81.2 .232

2135.
d29.
19.7
8.7
9201.



I5d3. 7.d3 .285
216. .336 2.13
13.9 d.5l 2dl.
90.1 8.3 15. d
Ml 9 It
1* * 3
66d9. 32.0 1.23


203.
215.
55.5

9
dd.7

12.2
26.)
13d.
9-5
d2
132.

10.3
15.9
III.
d.2
dd.5
d*c
e£
.087 .057
.122 .162
85.8 151.

8 3
.019 .013

.03d .019
.112 .023
137. 106.
12 7.d
25 27
.369 .203

.OdS .015
•Sd9 .0)6
273. 8d.B
Id. 3
Ui »
i j
.I9d .063
• percentage of
.01



5
.OOd

.Oil
.OOd
36.1

31
.115

.Oil
.Od6
205.8
5.9
.01.8







.Old
.Old
82.9

17
.Id7

.015
.Oil
62.3
10
1 A
III
.063
105. 768.
86. d d09.
67.2 1.7.5
66.7
5 6
23.1 169.

19.7 d03.
30.6 65.5
d.3 16.0
11.8 83.)
17 IB
213. d35d.

13.0 503.
10. 1 9d.3
66.1 18. d
22.2 8d.6
Si j
13
55.9 2I6B.
232. 627.
29.9
12.8
100
5 1
95.2 257.

237. 196.
37.8 29.7
15.7 15.0
9d.l 90
17 10
2561. 2120.

123. 225.
13.3 7d.d
10.7 31.5
100 100
530. 971.
266.


100
1
109.

lie.
7.6d
6.dd
90
10
I26o.

75.6
18.2
23.6
100
326.
30.


100
1
12.3

13.0
5.10
36.6
90
10
Idl.

15.2
9.d2
55.3
100
65.6
28.7
20.9
6d.B

2
6.32

126. 7.27
53.6 3.28
39.9 d2.0
68.9
9 H
1361. 78.6

79.2 d.63
8.71 1.78
10.9 35. d
100 33.3
3dl. 20.0
composite sample In total sampling effort
• number of quality determination made for the
parameter



       CCV - coefficient of variation
kg/ha* mass In kg/ha for material  Intercepted by  the unit

-------
rv
-j
                                                                          TABLE    0-1


                                                                               CONT.
SUURCE ALK
(09 CaCOj/l)
HANCOCK
COND TOS pll TKN
(u9/l) (ng N/l)

fclfl /MA
n\tn 1 (11*1
(«9 N/l)

NII3 TOTAL P
(ogN/l) (»g P/l)


ORTIIO P ORG.P
(•19 P/D <«>9/P)

COO Cl
(P9/D ("9/1 )

SO. Ca
(ug/l) (HCJ/I)

WO

K

Na

TOC
(«9/D

TUBE 113-114 DEPTH AVERAGE
G* 333.
S0b 77.9
CVC 22.9
ICd 75
Ee 12
kg/haf 25i4.
TUBE 121
G 392.
SO 52.4
CV 13.3
1C 50
E 12
kg/ha 6708.
TUBE 122
G 30J.
SO 1,9.8
CV li.3
« 27.3
E II
kg/ha 1,699.
aG - geometric mean
bSD - standard deviation
2096. 1492. 7.48 .279
337. 152. .372 1.37
15.9 4.2 4.97 227.
8.1 85.7 2.9 15.2
62 28 34 33
15846 11283 56.5 2.12

1816. 1056. 7.49 .133
278. 211. .231 .292
15.2 19.4 3.09 III.
4.3 59.3 7.1 13.8
46 27 26 29
31114 18095 128. 2.27

1691. 1014. 7.61 .186
246. 164. .262 .316
14.4 16.0 3.43 104.
4.9 57.1 9.5 14.3
41 21 24 21
26257 15746 118. 2.89


11.5
23.0
130.
7.6
66
86.9

.387
26.5
391.
6.2
49
6.63

.236
8.63
291.
7.5
4o
3.67
d«C
eE
.038
.342
244.
12.8
39
.284

.017
.048
143.
II. 8
34
.301

.016
.052
169.
11.5
26
.253
.017
.021
101.
5
40
.131

.016
.043
163.
2.9
35
.274

.015
.021
101.

28
.233
• percentage of
.Oil .014
.028 .012
184. 74.5
2.1 3-7
48 27
.082 .106

.Oil .013
.004 .016
39.6 95.3
2.4
40 24
.199 .233

.013 -013
.165 .018
389. 108.
6.25
29 16
.200 .203
conpotl'tc sample
17.0 442.
25.8 93.2
112. 20.6
15.4 83.9
26 31
129. 334).

19.4 267
19.0 68.4
64.2 24.8
21.1 66.7
19 27
332. 4574.

18.0 257.
44.5 160.
147. 54.7
12.5 58.3
16 24
280. 3396.
183. 207.
65.0 52.7
33-5 24.8
96.4 93.8
28 16
1385. 1562.

189. 187.
23.3 47.1
12.3 24.0
95 90
20 10
3232. 3206.

216. 157.
51.9 30.7
23.6 19.1
71.4 67.5
14 8
3362. 2444.
too.
23.9
22.6
93.8
16
757.

78.2
7-96
10. 1
90
10
1340.

65.6
7.54
11.4
87.5
8
1019.
13.8
6.89
45.7
93.8
16
104.

21.5
6.05
27.3
90
10
368.

16.1.
5.42
31.6
67.5
8
255.
107.
50.3
43.8
92.9
14
807.

106.
10.4
9.76
86.9
9
1817.

107.
13.5
12.5
65.7
7
1657.
6.20
3.09
45.4
it. a
17
46.9

6.94
10.5
107.
26.7
15
119.

4.04
2.28
50.6
23.1
13
62.7
In total sampling effort
• number of quality determination made for the
parameter




        £CV - coefficient of variation
kg/lia- mass In kg/lia for material  Intercepted by  the unit

-------
                                                                      TABLE   0-1
                                                                         COHT.
ro
00
SOURCE ALK CONO IDS pll TKN
(»j CaC03/l) (og/l) (»g N/l)
HANCOCK


N02/H03 Nil-, TOTAL P OKI 110 t ORG.P COD Cl SO^
("9 N/l) (») N/l) («ig P/l) (mg P/l) (mg/P) (pg/l) (ug/t) (my/I)




Ca
(«9/U

HO

K

Na

TOC

TUBE 121-122 DEPTH AVERAGE
G1
sob
CVC
K
E8
kg/haf
TUBE 123
u
SO
CV
1C
E
kg/ha
TE -24
SI)
CV
»c
E
kg/ha
aG •• geometric
bSU • standard
346.
67.3
19.1
39
23
565.

272.
74.9
26.6
*2.9
14
3082.
237.
29.9
12.6
50
10
24)5.
wean
1756. 1038. 7.5* .153
270. 192. .252 .300
15.2 18.2 3.3* 107.
4.59 58.3 7.69 1*
87 48 52 50
28676 169*3 123. 2.50

1627. 99*. 7.68 .197
53*. «*7. .37* .502
31.7 14.6 4.86 116.
3.9 68.2 6.4 20.7
SI 22 31 29
18431 11260 87.0 2.23
1419. 90S. 7.55 .195
277. 73.4 .319 .788
18.9 8.13 4.23 193.
4.2 65.2 10.3 20
48 23 29 30
16306 10398 86.8 2.24

.310
20.5
405.
7.9
89
5.06

2.52
97.1
239.
11.8
SI
28.6
.521
41.6
265.
13.7
51
5.99
dic
deviation E
CCV • coefficient of
variation
fkg/ha
.017 .016
.0*2 .035
152. 1*7.
11.6 1.6
60 63
.278 .261

.028 .016
.091 .016
1*5. 83.
16.7 2.8
36 36
.317 .177
.022 .016
.19* .028
293. 122.
17.1 6.25
35 32
.253 .180
- percentage
• number of
.Oil
.107
443.
1.4
69
.181

.Oil
.006
5*.B
2.6
38
.127
.012
.021
128.
5.3
38
.140
.013 18.7 262. 199.
.016 32.9 119. 40.2
94.1 126. 42.1 19.8
2.5 17-1 62.7 85.3
40 35 51 34
.219 306. 4285. 3260.

.014 32.3 246. 147.
.012 46.3 51.7 23.5
74. a 94.0 20.5 15.8
S.5 42.1 68. 80
18 19 25 15
.157 366. 2789. 1671.
.014 34.5 241. 134.
.021 173. 50.8 25.2
113. 194. 20.6 18.6
5.0 31.6 64 60
20 19 25 15
.162 396. 2769. 1534.
173.
43.5
24.1
BB.8
18
2830.

120.
18.7
15.4
80
10
1358.
117.
24.5
20.6
75
8
1349.
72.3
9.92
13.6
8.B8
18
1181.

82.0
6.33
7.69
20
10
929.
56.9
6.94
12.1
25
8
655.
19.1
5-17
30.9
88.8
18
312.

25.3
4.75
18.5
80
10
287.
14.5
3.42
23.1
75
8
166.
106.
11.4
10.7
87.5
14
1736.

99.2
29.1
28.3
77.8
9
1124.
106.
29.5
27-2
75
8
1209.
5.39
8.14
III.
25
28
88.1

7.92
5.58
60.0
38.5
13
89.7
8.07
14.17
118.
30.8
13
92.7
of compotlte sample In total sampling effort
quality determination wade for the parameter
• mass In kg/ha for iialcrU) Intercepted by the unit

-------
ro
10

SOURCE AlK
(iq CaCOj/1)
HANCOCK

COND TDS pll TKN
(ug/l) (OK, N/l)


9.7 102. 7.99
20.8 14.2 6.92 28.5 10.6
17.3 20.0 33.2 27.1 100.
77.8 77.8 77-8 76.5 34.6
18 18 IB 17 26
1355. 793. 225. 1164. 91.2

23.4

100

1.87







aG  - geometric iioan
bSD - standard deviation
CCV - coefficient of variation
                                                                kg/ha
percentage of compos It* sample In total sampling effort
number of quality determination made for tlie parameter
mass In kg/ha for uaterlal Intercepted by the unit

-------
                                                                              T A B I E    0-1


                                                                                   CONT.
SOURCE      AU     COND  TOS   pll   fitfi

       (09 CaCOj/l)      (ag/l)    (ig M/l)  («HJ  N/l)  (09 N/1)  (ing P/l) (ing P/l)
NOyNOj   ffilj    TOTAL P  ORTliO P  OnS.P   COO    Cl
                                                         SO
                                                                                                              Ca
                                                                                                                       ^           Hg

                                                                                                      (P9/U ("9/D ("9/0 ("il/0 ("9/D
                                                                                                                             K      Na    TOC

                                                                                                                                  (•wj/0 ("9/0
               HANCOCK
              TUBE  211
                a
               c
               so"
               cvc
                     3570.
9.17
                                                                        .01
               kg/h«
                                                                                      .000$
OJ
o
TUBE 2U
 o
 SO
 cv
 sc
 E
 kg/ha
                                                8.08  5.25    27.0
                                                1.13  .735
I
3.78
          .025
          .007
          28.3

         . 2
          .003
                                                                       .022
                                                                       .028
                                                                      9
-------
TABLE    D -  I




     CUNT.
SOURCE ALK
(ng C.CO.,/1)
HANCOCK
TRAY 302
6»
sub
CVC
xcd
Ee
kg/haf
TRAY 303
G 2 1.6.
SO
CV
1C
E 1
kg/ha 95.9
CONU 70S pH TKN HOj/NOj NHj TOTAL P
(tng/l) (mg N/l) (ng N/l) (ing N/l) (mg P/l)


1234.
Sili.
1.2.6

6
370.









7.00



1
2.1

1402. 7.80



1 1
5*7. 3.04


.527
1.90
132.
50
2
.158

.692
.600
61.9
40
5
.269


11.2
76.3
159.
33.3
3
3.40

9.19
9.75
81.2
30
10
3.58


.107 .01
.332
140.
33.3
3 1
.032 .003

.061 .01
.086
79.3
50
6 1
.024 .004
ORTKO P ORG.P COD
(«g P/l) 
-------
                                                                     TABLE
                                                                                 D - I
                                                                          CONT.
00
ro
SOURCE AU COND TOS pi! TKN
(•9 CaC03/l) («g/1) (mg N/l)
HANCOCK
TUBE 314
G* 600. .79
so"
c»c
xcd too
Ee | |
kg/ha ,8 02^
TUBE 313-314 DEPTH AVERAGE
<• 2046. .199
SO 646. .398
CV 29.4 121.
XC 66.7
E II 3
kg/ha 246. .024
G
SO
CV
XC
E
kg/ha
*G • geometric mean
SO • standard deviation
£CV - coefficient of variation
N02/N03 WI3 TOTAL P
<«g N/1) («ig N/l) (ng P/l)


3.22 .170
3.52 .085
86.7 47.1
33.3 100
3 2
.097 .005
78.5 .088 .01
72.6 .091
51.5 79.2
20 75
15 4 4
9.42 .Oil .002






1C • percentage of
ORTHO t ORG.P COO Cl SOj Ca Mg 1C Ha TOC
(ng P/l) («g/P) (pg/l) (>ig/l) (uig/l) (mg/1) (»g/l) (mg/l) (wy/l) (my /I


45.8 28.
28.J
56.6
100 100
2 1
1.38 .18
.012 .01 51.2 63.3 243. 15.9
.008 21.6 81.3
55.1 39.5 95.1
100 100 100
74321 1
.003 .002 6.15 7.59 48.6 ).|8






coraposl trample In total sampling effort
eE • number of quality determination nade for the parameter
kg/ha- mass In kg/ha
for naterlal Intercepted by the unit

-------
co

SOURCE ALK COND TOS pi! TKN
(rag CaC03/l) (mg/1) (09 N/l)
HANCOCK
TRAY 304
G* 1160. 1039.
SDb
CVC
xcd
te II
k9/ha . 81.2 7.27
TRAY 305
G 214. 1177. 7-08 .10
SO 101.
CV 8.60
XC
E l 3 II
k9'ha 68.5 377. 2.27 .0)2
TRAY 306
G
SO
CV
XC
E
kg/ha

N02/N03
(ng N/l)


1.22
.849
62.4

2
.086

2.11
9.46
152.
33.)

.676

.27



1
.024
TABLE D - 1
CONT.
NH3 TOTAL P ORTIIO P ORG.P COO Cl SO^ Ca Hg K Na TOC
(«g N/l) (ng P/l) (Big P/l) (ng/P) (pg/l) (og/l) («g/l) (ng/l) (ng/l) .(uig/l) (ng/l) (.ig/0


.305 .024 1.26
.332 .035
86.3 101.
SO 100
2 2*1
.021 .002 .088

.01 .018 .03 H7.



Ill 1
.003 .058 .001 37.4

.08 .07



1 1
.007 .006
          °so
geometric mean
standard deviation
          CCV • coefficient of variation
 XC   * percentage of compot I te tamp!*  'n tout sampling effort
e£    * number of quality determination Mde for the parameter
fkg/ha- mass In kg/ha for material  Intercepted by the unit

-------
                                                                            TABLE     0-1

                                                                                 COHT.
CA)
SOURCE AU COND TDS pll TKN
(ng CaC03/1) (og/1) (ng H/l)
HANCOCK
TRAY 304-306 DEPTH AVERAGE
G" 214. 117). 10)9. 7.08 .10
Sl)b . 83.5
CVC 7. 1
tt"
Ee 1 4111
kg/ha je.S IBS. 166. 2.27 .032
TRAY 307
G 2.83
SO
CV
E 1
kg/ha .198
TRAV 308
G
SO
CV
1C
E
kg/ha
NOyMOj NHj TOTAL P ORTHO P ORG.P COD Cl S04 Ca Hg K Ma TOC
(ng N/l) (ng N/l) >g P/l) (ng P/l) (og/P) (pg/l) (ng/l) («g/l) (ng/l) (.ug/1) (ng/l) (ng/l) (ng/
1.25 .092 .18 .034 * 1.26 117. . ' •
6.65 .276 .028
IBS. 129. 64.8
16.7 25 100
6 4 1 4 II
.199 .015 .058 .005 .088 37.4
16.6 .)) 1)1. 67. 35.7 10. 79.
II 1 1 1 1 1
1.16 .023 9.17 4.69 2.49 .7 5.53
.27 .6) .01
1 1 1
.078 .18) .00) '
            G  • geometric nean
            SO - standard deviation
           CCV - coefficient of variation
d«   • percentage of C0mpo»lto  sample  In total sampling effort
e£    • nunber of quality detemlnatlon Bade for the parameter
fkg/ha- mass In kg/ha for tuterlal  Intercepted by the unit

-------
co
en
T A B L
CONT,
SOURCE ALK
(mg CaC03/l)
HANCOCK
TRAY 309
6«
so"
CVC
«c<
Ee
kg/haf


261.



1
20.9
COHO


1005.
81.4
8.09

3
80.4
IDS
("9/1 )


905



1
72.4
pH TKN NOj/NOj Nllj
(ng N/l) (mg N/l) (og N/l


7.38 .279
.225 .481
3.05 109.

3 2
.591 .022


.915
.687
63.8

3
.073


.02
.017
69.3

4
.002
E 0 -
I
TOTAL P ORTHO P ORG.P
) (n>9 P/l) (ng P/1) («9/P)


.01



2
.0008


.020
.019
76.6

4
.002


.01



I
.0008


COD Cl S04 Ca Mg K Na TOC
(pg/D («g/D («9/D («g/D («g/U («g/U («9/D («g/<


24.



i
1.92








TRAY 307-309 DEPTH AVERAGE
G
SD
CV
1C
E
kg/ha
TUBE 311
G
SO
CV
1C
E
kg/ha
8G • geometric
bSD • standard
26).



1
20.9

121.
11.3
9.35
100
2
130.4
mean
deviation
1005.
81.4
8.09

3
80.4

2397.
271.
11.3
14.3
14
2589.
905



1
72.4

1615.
553.
33.0
too
3
1743.
7.38 .604
.225 1.42
3.05 115.

3 3
.591 .091

7.75 .808
.120 .198
I.S5 24.1
100 100
2 2
8.37 .873
1.28
7.04
175.

5
.192

41.2
4.67
11.2
14.3
14
44.5
.057
.253
.143.

6
.009

.153
.035
22.8
100
2
.165
.01



2
.0008

.013
.020
112.
100
6
.015
XC * percentage



«£
- number of
• 017
.018
81.3

5
.003

.01



7
.Oil
.01



1
.0008

.013
.012
81.6
. 100
6
.014
Of composite sample
quality
56.1 67 35.7 10..
75.7
97.6

2 III
8.41 4.69 2.50 .7

2.12 421. 63.5
31.7 122. 17-1
141. 28.2 26.3
100 100 100
2 3 3
2.29 454. 68.6
In total sampling effort
79.



1
5.53

5.35
.212
3.96
100
2
5.78

dateralnatlon made for the parameter
         CCV - coefficient of variation
'kg/ha- nass In kg/ha for material Intercepted by  the unit

-------
CO
Cft

SOURCE ALK
(ng CaC03/l)
HANCOCK
TUBE 312
G*
SDb
CVC
Kd
Ee
kg/haf

COND TDS
("9/0


1527.
336.
21.3

9
183.

pH TKN
("9 N/l)


1.7*


100
I
.209

N02/N03
(*g N/l)


77.0
10.0
12.9
10
10
9.24
TABLE
CONT,
Nllj TOTAL P
(ng N/l) (ng P/l)


.08 .26


100 100
1 1
.009 .031
D
- I
ORTHO P ORG.P COD Cl
(og P/l) («9/P) (pg/l) (ng/l


.01



3
.001


112 1.50


100 100
1 1
13.* .18

S04 Ca Hg


184


100
i
22.1

K Na IOC


27.1


100
1
3.25
TUBE 311-312 DEPTH AVERAGE
G 121.
SD 11.3
CV 9.35
xc 100
E 2
kg/ha 130.
TUBE 313
G
SD
CV
SC
E
kg/ha
*G • geometric man
bSD • standard davlatlon
2009. 1615.
509. 553.
24.4 33.0
8.7 100
23 3
1206. 1744.

2313.
391.
16.6

10
463.


7.75 1.03
.120 .5*9
1.55 48.B
100 100
2 3
8.37 .617

.01


50
2
.002


CCV • coefficient of variation
53.5
19.6
34.6
12.5
2*
32.1

17*.
17-8
10.2
8.3
12
34-9
d«C
•E
.123 .021
.05 .093
38.5 176.
too too
3 7
.07* .012

.0*6 .01
.028
56.6
50
2 *
.009 .012
- percentage of
.01



10
.006

.013
.008
55.1

7
.003
.013 7.96 325.
.012 56.3 173.
81.6 108. 47.7
100 100 100
6 3 4
.014 4.78 195.

.01 64. 143.

•
100 100
4 1 1
.002 12.8 28.6
82.9
61.1
64.5
too
4
49.7

243.
i


1
48.6
9.19
12.6
99-7
100
3
5.51

15.9


100
1
3.18
compo* 1 tt sanple In total sampling effort
• nunber of quality
kg/ha* nass In kg/ha
for
deternlnatlon nade for the parameter
naterlal Intercepted by
the unit


-------
                APPENDIX E



EQUIVALENT RATIOS FOR WATER CHARACTERISTICS
                     137

-------
                                        TABLE E-l

                       EQUIVALENT RATIOS  FOR  WATER CHARACTERISTICS
                          ON THE BERMUDA PLOT AT THE GRAY SITE

Ratio
:o42"/cr
HCO,"/C1~
ca2+/cr
HC03"/Na*
K+/Na+
Ca2W
Mg2W*
SARa
Cl" - Na*
Cl"
BASE .
EXCHANGE0
Irrigation
.528
.692
.481
.531
.045
.369
.878
13.64
-.303
-'BA
Tray
61
.357
.094
.298
.129
.027
.411
.984
Depth
122
.374
.177
.312
.227
.016
.577
.735
23.08 23.23
.275
+ IBA
.218
+IBA
(cm)
183
.268
.183
.353
.241
.013
.464
.841
20.05
.241
+IBA
122
.294
.478
.441
.287
.009
.264
.613
38.50
-.668
-'BA
Tube Depth
183
.321
• .346
.367-
.348
.022
.369
.530
21.40
.006
•',.
(cm)
224
.489
.240
.573
.208
.011
.496
.320
28.13
-.154
-<=,
Ground
Water
.502
.596
.423
.563
.038
.400
1.45
12.38
-.058
-'BA
aSAR = NaV((Ca2+'+ Mg2+)/2)'[9.4-p(K2'-K1' )-p(Ca+Mg)-p(A1k)]

b-IBA meq/1 Cl" < meq/1 Na*  or  meq/1  (HC03" + S042")  > meq/1  (Mg2+ + Ca2*)

 +IBA meq/1 Cl" > meq/1 Na+  or  meq/1  (HC03" + S042")  < meq/1  (Mg2* + Ca2+)
                                       138

-------
                                         TABLE  £-2

                       EQUIVALENT RATIOS FOR WATER CHARACTERISTICS
                           ON THE COTTON PLOT AT THE GRAY SITE

Ratio Irrigation
jO^'/Cl" ..528
liCO-j'/Tl" .692
Ca2*/Cl~ .481
HC03"/Na*
Ca2W
Tray Depth (cm)
61 122 183
.366
.205
• .359


Tube Depth (cm) Ground
122 183 224 Water
.194 .602
.070 .596
.054 .423


              .878
                             .670
.271
                                                                                1.45
SAR
   Cl
BASE    h      ,
EXCHANGE0     ~'BA
                               BA
                                                     +I
  BA
aSAR
                    Mg2+)/2)i[9.4-p(K2'-K11)-p(Ca+Mg)-p(Alk)]
  -IBA raeq/1  Cl" < meq/1  Na+   or  meq/1  (HC03"  +  S042")  > raeq/1  (Mg2+ + Ca2+)

  HBA meq/1  Cl" > meq/1  Na+   or  meq/1  (HCOj" .+  S042")  < meq/1  (Mg2* + Ca2+)
                                        139

-------
                                      TABLE  E-3

                     EQUIVALENT RATIOS FOR WATER CHARACTERISTICS
                      ON THE  GRAIN  SORGHUM  PLOT AT THE GRAY SITE
Ratio
V-'/cr
HC03"/CT
Ca2*/Cl'
HC03*/Na+
Kf/Na*
Ca2W
M92+/Ca2*
SAR3
Cl" - Na*
Cl"
BASE .
EXCHANGE0
'SAR . Ma
b ,
Irrigation
.528
.692
.481
.531
.045
.369
.878
13.64
-.303
-'BA
,V((Ca2+ , ^2

Tray
61
.289
.312 .
.535
.220
.036
.378
.688
18.48
-.417
-  roeq/1 Na*  or  meq/1  (HC03"  * S042") < meq/1 (Mg2+ + Ca2*)
                                     140

-------
                                       TABLE  E-4

                     EQUIVALENT RATIOS FOR MATER CHARACTERISTICS
                       ON THE BERMUDA PLOT AT THE HANCOCK SITE
Ratio
•V'/cr
nco3"/ci"
ca2+/cr
HC03~/Naf
K*/Na+
Ca2W
Mg2t/Ca2+
SARa
Cl" - Na*
Cl"
BASE h
EXCHANGE0
aSAR = Na
Irrigation
.457
.738
.309
.507
.034
.212
.690
20.08
-.457
-'BA
+/((Ca2+ + Mg2*)/:
-IBA meq/1 Cl" < meq/1 Na
Tray Depth (era) Tube
51 122 183 122
.122 .223
.100 .118
.639 1.445
1
.
2.
.523 .703
4
'
+IBA +IBA . <
2)i[9.4-p(K21-K11)-p(Ca-t^g)-p(Alk)]
Depth (cm)
183 224
305
533
827
.43
076
217 •
799
.32
627
"„

Ground
Water
.903
2.54
1.03
1.39
.065
.565
1.71
5.49
-.827
-'BA

+ or meq/1 (HC03~ + S042*) > meq/1 (Mg2* + Ca2+)
+IBA meq/1  Cl" > meq/1  Na+   or   raeq/1  (HC03"  *  S042")  < meq/1  (Mg2+  + Ca2+)
                                      141

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                                         TABLE E-5

                        EQUIVALENT RATIOS FOR WATER CHARACTERISTICS
                          ON THE COTTON  PLOT AT THE HANCOCK SITE
Ratio     Irrigation
                                 Tray Depth (cm)
                               61     122      183
                                                     Tube Depth (cm)     Ground
                                                 122      183      224    Water
iicn3"/.ci
             .457

             .738
                       .483

                       .396   1.30
.188

.263
                                                                .284
.903

2.54
                                              1.52

                                              .075
                                                                                1.39

                                                                                .065
Ca2+/Na + .212 .972
Mg /Ca . .590 .88
SARa 20.08 4.55
Cl' - Na +
BASE h
EXCHANGE
.565
1.71
5.49

 aSAR = Na*/((Ca2* +  Mg2'l')/2)^9.4-p(<21-<1 ' )-p(Ca+Mg)-o(A1k)]

 b-IBA meq/1  Cl" < raeq/1 Na*  or  meq/1 (HC03" + S042") > meq/1 (Mg2+  * Ca2+)
meq/1 C1" > meq/1 Na*  or  meq/1 (HC03" + S042")  < meq/1 '(Mg
                                                                   2+
                                                                        Ca
                                                                          2*
                                         142

-------
                                        TABLE E-6

                       EQUIVALENT RATIOS FOR  WATER CHARACTERISTICS
                         ON THE CONTROL PLOT  AT THE HANCOCK SITE

Tray Depth (cm) Tube Depth (cm) Ground
Ratio Irrigation 61 122 183 122 133 224 Water
V'«-
nco3'/cr
Ca2+/Cl~
HC03"/Na+
ItW
Ca2W
Mg2+/Ca2+
SARa
C1" - Na+
cr
BASE h
EXCHANGE0
.543
.571
.343
.412
.247
.792
12.89
-.386
-'BA
.568
.935
1.162
1.50
.109
1.87
.698
4.65
.378
+IBA
.420
.742
.870
1.16
.114
1.36
.833
4.69
.362
+ IBA
.903
2.54
1.03
1.39
.065
.565
1.71
5.49
-.827
-'BA
"SAR - Naf/((Ca2+ + Mg2*)/2)*[9.4-p(K2'-K1l)-p(Ca+Hg)-p(Alk)]

b-IBA meq/1 Cl~  < meq/1 Na*  or  meq/1  (HC03" + S04Z") > weq/1  (Mg2+ + Ca2*)

 +IBA meq/1 C1~  > raeq/1 Na*  or  meq/1  (HC03* + S042") < meq/1  (Mg2* » Ca2+)
                                      143

-------
             APPENDIX  F

MASS INPUTS IN APPLIED WASTEWATER AND
    MASS OUTPUTS IN PERCOLATE AND
           CROPS HARVESTED
                 144

-------
                   TABLE  F-l

MASS INPUTS AND OUTPUTS IN KG/HA ON THE BERMUDA
 PLOT AT THE GRAY SITE OVER THE PROJECT PERIOD

Tray Death
Parameter
A.LK
TOS
TKN
N02+N03-N
NH3-N
TOTAL P
ORTHO P
ORG. P
COD
Cl
SO,
•»
Ca
Mg
K
Na
TOC
Applied
Wastewater
4170
18980 •
159
49.0
38.8
56.5
32.5
2.43
1650
2080
3040
1150
623
274
3610
548
61 cm
135
2840
.862
.949
.031
.177
.015


1020
491
171
102
21.9
736

122 cm
71.6
717

.568
.006

.001

9.0
286
53.7
36.5
16.3
2.02
145

183 cm
85.7
905
.087
9.01
.017

.004

13.5
. 332.
121
66.1
33.7
3.88
163

Tube Depth
122 cm
1160
5280
1.49
3.61
.045
.127
.152
.025
65.6
1720
6S7
429
160
28.2
1860
26.2
183 cm
411
2580
.595
1.31
.044
.044
.016
.032
70.4
841
366
174
56.1
19.9
542
26.0
244 cm
744
2440
1.28
13.49
.1.25
.036
.036
.027
81.7
2200
1460 •
712
138
32.2
1650
44.4
Crop


147


19.5



73.7
130
31.6
13.3
86.5
6.06

                   145

-------
                   TABLE  F-2

MASS INPUTS AND OUTPUTS IN KG/HA ON THE COTTON
 PLOT AT THE GRAY  SITE OVER THE  PROJECT PERIOD

Parameter
ALK
TDS
TKN
N02+N03-N
NH3-N
TOTAL P
ORTHO P
ORG. P
COO
Cl
SO,
t
Ca
Mg
K
Na
TOC
Applied
Wastewater
1730
' 7850
65.7
20.3
16.1 '
23.4
13.4
1.0
681
861
1260
476
258
113
1490
227
Tray Depth
61 cm 122 cm 183 cm
141
2090
1.68
7.20 .014
.050 .009 .011
.088
.089 .036 .002
.439
34.5
485 '
241
98.5
40.0
95.2

14.8
Tube Depth
122 cm 183 cm 244 cm
117 7.84
2760 95.0
.464
5.32 0.60
.044
.008 _
.012 .001

39.3
1170
309
327
53.7
7.54

8.72
Crop


16.8


2.44



.26
38.0
4.92
2.99
9.95
.317

                  146

-------
                      TABLE F-3

MASS INPUTS AND OUTPUTS IN KG/HA ON THE GRAIN SORGHUM
    PLOT AT THE GRAY SITE OVER THE PROJECT PERIOD

Tray Depth
Parameter
ALK
TDS
TKN
N02+N03-N
NH,-N
W
TOTAL P
ORTHO P
ORG. P
COD
Cl
SO,
Ca
Mg
K
Na
TOC
Applied
Wastewater
2000
9110
76.2
23.5
18.6
27.1
15.6
1.17
790
980
1460
552
299
131
1730
263
61 cm
462
3250
1.34
9.92
.132
.236
.129
.039
70.4
1050
410
318
132
58.5
964
45.6
122 cm

807

.500
.027

.019
22.6
12.9
352
120
51.0

10.8


183 cm
52.6

.248
.102
.012
.004
.055
.001
21.2
17.2
25.3
7.74
1.72
6.45


Tube Depth
122 cm
280
2910
.58
9.77
.047
.023
.021
.026
21.4
899
468
265
107
39.2
39.4
6.1
183 cm 244 cm
712
7570
1.16
11.5
.111
.037
.041
.030
97.9
2350
1470
1520
268
26.2
1690
25.8
Crop


29.5


5.82



2.90
19.9'
4.90
4.21
9.27
0.59

                      147

-------
                      TABLE F-4

MASS INPUTS AND OUTPUTS IN KG/HA ON THE BERMUDA PLOT
    AT THE  HANCOCK SITE OVER THE PROJECT PERIOD

Tray Depth
Parameter
ALK
TDS
TKN
N02+N03-N
NH3-N
TOTAL P
ORTHO P
ORG. P
COD
Cl
so4
Ca
Hg
K
Na
TOC
Applied
Wastewater
8680
29620
940
2.85
52.1
359
207
6.67
6120
8300
5070
1450
607
455
7870
1365
61 cm 122 cm
116
1971
.314
1.38
.041
.016
.011

46.3
817
135
295
93.8
13.2
26.8
8.45

247

10.1
.016

.001

4.5
60.3
39.9
30.5
21.2
3.12


Tube Depth
183 cm 122 cm 183 cm 244
52.5
2130 •
.187
44.7
.019
.013
.004

23.1
169
95.2
257
109
12.3

6.32
2510
11282
2.11
86.9
.284
.131
.082
.106
128.8
3340
1380
562
757
104
807
46.9

cm Crop


229


31.6



. 39
238
41.2
18.6
116
10.8

                      148

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                    TABLE F-5

 MASS INPUTS AND OUTPUTS IN  KG/HA ON THE COTTON
PLOT AT THE HANCOCK SITE OVER THE PROJECT PERIOD

Tray Depth
Parameter
A.LK
TDS
TKN
N02+N03-N
NH3-M
TOTAL P
ORTHO P
ORG. P
COD
CV
SO,
•t
Ca
Mg
K
Na
TOC •
Applied
Wastewater
4870
16630
527
1.60
293
201
116
3.74
3440
4660
2850
813
341
255
4420
766
61 cm 122 cm
95.9 68.5
547
.224 .032
3.38 .199
.026 .015
.004 .058
.006 .005

17.1 .088
154 37.4
112




6.19
183 cm
20.9
72.0

.192
.009
.008
.003
.008
8.41


4.69
2.50
.700
5.53

Tube Depth
122 cm
130
1740
.617
32.1
.074
.012
.006
.014
4.78
195
49.7




5.51
183 cm 244 cm


.024
9.42
.011
.002
.003
.002
6.15
7.59
48.6




3.18
- Crop


12.3


1.70



.569
32.9
3.53
2.47
10.6
.190

                     149

-------
                      TABLE p-6

MASS INPUTS AND OUTPUTS IN KG/HA ON THE GRAIN SORGHUM
   PLOT AT  THE  HANCOCK SITE OVER THE PROJECT  PERIOD

Parameter
ALK
TDS
TKN
N02+N03-N
NH3-N
TOTAL P
ORTHO P
ORG. P
COD
Cl
so4
Ca
Mg
K
Na
TOC
Applied
Wastewater
1970
6730
214
.647
118
81.5
47.0
1.52
1390
1890
1150
329
138
103
1790
310
Tray Depth Tube Depth
61 cm 122 cm 183 cm 122 cm 183 cm 244 cm Crop


.171 .735 141
.40 .165 1.62 3.78
.011 .003
.002 .001 .001 .003 26


4
35.1
71.0 377
27
27.4
94.6
2.78
1.87
                      150

-------
                      TABLE  F-7.

MASS INPUTS AND OUTPUTS IN KG/HA ON THE CONTROL PLOT
     AT  THE  HANCOCK  SITE OVER THE  PROJECT  PERIOD

Parameter
ALK
TDS
TKN
N02+N03-N
NH3-N
TOTAL P
ORTHO P
ORG. P
COD
Cl
so4
Ca
Mg
K
Na
TOC
Applied
Water
3270
15100

1.78





4030
2960
770
381

3640

Tube
122 cm
5650
16900
2.49
5.06
.278
.261
.181
.219
306
4300
3260
2830
1180
312
• 1736
,88.1
Depth
183 cm
2930
10800
• 2.24
13.1
.285
.178_
.133
.159
381
2780
1600
1350
793
225
1163
91.2
Crop


123


1.70



.569
32.9
3.53
2.47
10.6
.190

                        151

-------