PB-229  660

BACKGROUND  INFORMATION  FOR  PROPOSED NEW SOURCE
PERFORMANCE  STANDARDS:  ASPHALT CONCRETE PLANTS,
PETROL-BUM  REFINERIES,   STORAGE  VESSELS,   SECONDARY
LEAD  SMELTERS AND  RE FINE RIE S, BRASS  OR  BRONZE  INGOT
PRODUCTION  PLANTS,  IRON  AND STEEL  PLANTS,   SEWAGE
TREATMENT  PLANTS:  VOLUME  II, APPENDIX: SUMMARIES  OF
TEST DATA

U. S.  Environmental  Protection Agency
Research Triangle  Park,  North  Carolina
                                                    DISTRIBUTED BY:
                                                    National Technical Information Service
                                                    U. S. DEPARTMENT  OF COMMERCE
                                                    5285 Port Royal Road, Springfield Va. 22151
                    This document has been approved for public release and sale.

-------
 BIBLIOGRAPHIC DATA
 SHEET
                  1. Report No.
                              APTD-1352b
                       PB   229   660
4. Tiile ind Subtle BACKGROUND INFORMATION FOR PROPOSED NEW SOURCE
PERFORMANCE  STAKDARDS:  Asphalt Concrete Plants, Petroleum Reflr
eries.  Storage Vessels, Secondary Lead  Smelters and?Refineries,
Brass or  Bronze Ingot Production Plants, Iron and Steel Plants,
7. Aiahor<»)
                     Sewage Treatment  Plants; Volume Z, Appen-
                     4jj$:  Summaries of Test Data      	
                                                              ft. Perioraia* Orgtaiutioa Re pi.
9. Performing Organization Name and Addles*
U.S. Environmental Protection Agency     ,
Office of Air and Water Programs
Office of Air Quality Planning and Standards
Research Triangle Park, North Carolina  27711
   Sponsoring Org«oii«tiofi Name and Addrei
                             Ieport D«tr
                              fr  June 1973
                                                              10. Project/Ta»k/Vork Unit No.
                                                              11. Conutct/Gruu No.
15. Supplememwx
            rUuiuiaent provides background information on the derivation of the propose
 second group of new source performance, standards and  their economic impact on the con-
 struction and operation of asphalt "concrete."plants, petroleum refineries, storage vesse
 secondary-lead smelters and refineries, brass or bronze ingot production plants, iron
 and steel plants,  and sewage.treatment plants.  Information is also provided on the en-
 vironmental impact of.Imposing the standards. 'The standards require control at a level
 .typical of well controlled existing plants and attainable with existing technology. To
•determine these levels, extensive on-slte* investigations were conducted, and design fac
 tors, maintenance  practices, available ,'test data*, and the character of emissions were
 considered.•^^epnomic analyses of Jthe^.e"f,fects"of .the  standards indicate th^^ll^joot
 cause undue reductions of profit .margins^'or reductions in growth rates. j|[ UrtiPappenJix
 presents summaries of. source testsrci'ted'in Volume 1. The summaries are concerned prii
 cipally with tests for particulate matter and carbon  monoxide, but also describe  the
 facilities.' characteristics of exhaust gas streams, and conditions of operation.
17. Key Wordi.«fld Docu
Air  Pollution
Pollution control             ;
* Performance standards
* Asphalt concrete plants :•
* Petroleum refineries
* Lead smelters and refineries ""
* Brass ingot production
*•< Bronze ingot production
* Iron production

ITb. Ueanfters/Opcn-Eaded Tern*

* Air pollution control
* Steel production
* Sewage treatment
17e- COSATI Field/Group
                              Reproduced by
                                NATIONAL  TECHNICAL
                               INFORMATION  SERVICE
                                U S Department of Commarc*
                                   SpringfiaU VA 22151
18. A«ftiiBbiiitr Stucawai On request from:
Emission Standards  and Engineering Division
Environmental Protection Agency
Research Triangle Park, North Carolina  27711
	ATTB:  Mr. Don-R. Goodwin-
'ONM MTt»S» INK*. *
                 9. Security Class (1
                   Report)
                     UNCLASS1FII
                    IJNCLA
                                                                       The APTD  (Air Pollution Technical Data) series  of reports is  issued by the
                                                                       Office of Air Quality Planning and Standards, Office  of Air and Water  Pro-
                                                                       grams  Environmental Protection Agency, to report technical data of interest
                                                                       to a. limited number of readers.  Copies of APTD reports are available  free
                                                                       of charge to Federal employees, current contractors .and grantees, and  non-
                                                                       profit organizations - as  supplies permit -  from the^Vir Pollution Technical
                                                                       Information Center, Environmental Protection Agency,  Research,Triangle Parx,
                                                                       North Carolina  27711 or nay be obtained, for a nominal cost, f ron .the
                                                                       National  Technical Information'Service, 5285 Port Royal Road, Springfield,
                                                                       Virginia   22151.
                                                                                                      AWBERC  OBRAR7
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                                                                                                    Publication No.  APTD-1352b
                                                                                                                                                 11

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                              TABLE OF CONTENTS
                                                                    Page

INTRODUCTION 	   1

HOT MIX ASPHALT CONCRETE PLANTS   	   3

PETROLEUM REFINERIES -  FLUID  CATALYTIC CRACKING UNITS   	  22
                                         y
SECONDARY LEAD SMELTERS AND REFINERIES .  .  .  . :	31

SECONDARY BRASS AND BRONZE INGOT PRODUCTION PLANTS  	  42

IRON AND STEEL MILLS -  BASIC  OXYGEN PROCESS FURNACES  	  52

SEWAGE TREATMENT PLANTS - SEWAGE SLUDGE  INCINERATORS  ........  60
                               111
                                  INTRODUCTION

     This appendix presents summaries of source tests cited in the
document.  The sumnaries are concerned principally with tests for
participate matter and carbon monoxide, but also describe the
facilities, characteristics of exhaust gas streams, and conditions
of operation.
     For each source category, facilities are identified by the same
coding used in the technical reports.  For example, Table A-16
summarizes results of the December 1971. test of petroleum refinery
catalytic cracking Facility A.  These results are also plotted as
Bar A, in Figure 3 of the Technical Report Number 7.  In this case,
the bar represents the range of the two valid results.  Table A-17
summarizes a second test, A,,, conducted in February 1972 at the same
facility.

     Most of the tests summarized herein were conducted using the
reference test methods of 40 CFR 60.- Wherever particulate tests
were conducted, additional measurements were made to evaluate
materials that condense and collect in impingers as the gases are
cooled to 70°F.  In the summaries, the "probe and filter catch" is
the particulate that relates to the standard and the EPA reference
method (Method 5 of 40 CFR 60 as published December 23, 197.1).   .
The 'total catch" includes the probe and filter catch, plus material
collected 4n the impingers using the particulate method as described
in 36 FR 15704, published on August 17, 1971.

-------
     Where particulate testing was  performed using methods other than
those cited above, the method ts  noted under "Facility" 1n the
discussion and also in the appropriate table.  Code test methods are
listed in the "Introduction"  of the main text.
                         HOT MIX ASPHALT CONCRETE PLAHTS

PARTICULATE TEST RESULTS
     Four hot mix asphalt concrete plants were tested by EPA,  one
controlled with a high-pressure-venturl  scrubber and three with
baghouses.  In addition, State and local control  agencies provided
data from the testing of four plants controlled with venturi
scrubbers and three with baghouses.   National  Asphalt Pavement
Association tests of four plants controlled with baghouses are
also included.  Two of these are not representative of "best
demonstrated technology" because poor collector maintenance or
operation was observed during testing.  Additional information
was available from an EPA study of asphalt concrete plants in
the Seattle, Washington, area.  The latter plants were not
necessarily well controlled and were tested to determine average
emission  factors.
     For  each plant, exhaust gases were analyzed after discharge from
the particulate collector.  These gases included drier exhaust gases
and sweep air used to gather dust at various points in the system
such as elevators, screens, and scavenger systems.  The front and back
half catches could not be separated (based on data supplied)  for Plants
F and G,  and therefore are comparable to the catch from the total £PA
train.
Facilities:

A,.  Oil-fired, 120-ton/hr design capacity, equipped with a cyclone
     and  a closed suction-type cyclic-cleaned baghouse designed for
     99.9+ percent efficiency.  Plant was operating at or near
                                   3

-------
     capacity for conditions prevalent during  the  test  periods.
A,.   Same location as plant A^   Gas-fired  rotary  dryer,  production
     rate of 115 tons/hr during  sampling, equipped with a cyclone
     and a baghouse.  -Opacity Was reported  to  be less than 5  percent;'
     Data' provided by^.the National  Asphalt  Pavement Association.
 '   .    '• '     *J  ;   £• *'  t; '   $;  :•>'     •      ?   '   "- '
B.  .  Oil-fired, 300-to^i/hr design capacity, equipped with a closed
   '  '    ;      ••   .'-•<-.',   '  :,-•'.'f-.               •
     suction-type cyclic-cleaned baghouse designed for  99.9+  percent
     efficiency?  Plant was operating at an estimated 80  to 90  percent
     capacity for conditions prevalent during  the  test  periods.

C.    Oil-fired, 200-ton/hr design capacity, equipped with a cyclone
     and a high-pressure venturi  scrubber operating at  20.4 inches of
     water pressure drop and approximately  14  gallons of  water  per
     1000 scfm of exhaust gases.   Data were provided by a local  control
     agency.  The plant was operating at approximately  70 percent and
     100 percent of design capacity during  the test periods.  No exhaust
     gas opacity readings were available.   The air flow rates (dscfm)
     for this plant were unusually high for a  typical 200-ton/hr plant.
     The plant was not observed  or tested by EPA.

D.    Gas-fired, 240-ton/hr design capacity, equipped with a multicyclone
     and a closed suction-type cyclic-cleaned  baghouse  designed  for  99.9+
     percent efficiency.  Plant  was operating  at or near  capacity for
     conditions prevalent during the test periods.

E.    Batch process, 180-ton/hr rated capacity, gas-fired, equipped with
     a multicyclone and a closed suction-type  cyclic-cleaned  baghouse
  .   designed for 99.9+ percent  efficiency.  Plant production during
     the test period is unknown.   Data were provided by a local control
     agency.   No exhaust gas opacity readings were available.

F.    Gas-fired, 250- to 300-ton/hr design capacity, equipped with a
           ' •**  ' ;   .   '-       - <  -                    ..,:;
     cyclone  and a closed suction-type cyclic-cleaned baghouse
    ^designed?for" 99.9+ percent efficiency.  Plantjroduction during
   '*£     '•          •'                 •            *•'.••>.-
     the test periods is unknown.   The_testing was performed and
              • •                         •          '        -' '
     data were provided by a local control  agency. : No exhaust gas
     opacity readings were available.
G.    Gas-fired, 75-ton/hr design capacity,  equipped with two cyclones   '
     and a high-pressure venturi  scrubber operating at 16 inches water
     pressure drop and approximately 11.5 gallons of water per 1000
     scfm of exhaust gases.  Tested.using Code Method 3.  Production
     rate during the test period was approximately 100 percent of
     capacity.  Data were provided by a local control agency.  No
     exhaust gas opacity readings were available.
H^  Oil-fired, 240-ton/hr design capacity, equipped with a cyclone
     and a high-pressure venturi  operating at 18.5 inches water
     pressure drop and approximately 18 gallons of water per 1000
     scfm of exhaust gas.  Plant was operating at capacity for
     conditions prevalent during the test periods.  Exhaust gas
     opacity readings were not recorded.

H£.  Same plant as Hj.   Testing conditions differed in that production
     rate was 200 tons/hr, the venturi scrubber was operating at  19.5
     inches water pressure .drop and the test results were provided by
     a local  agency.

-------
I.   Gas-fired, 120-ton/hr design capacity, equipped with a venturl
     scrubber operating at 26 Inches water pressure drop.  Plant
     production data during the test periods Is unknown.  Testing
     was performed and data were provided by a State control agency.
     No exhaust gas opacity readings were available.
J.   Baghouse collector.  Data provided by a State control agency.
     Operating conditions unknown.
K.   Oil-fired rotary dryer, production rate approximately 120 tons/hr,
     equipped with a cyclone and a baghouse.  Data provided by the
     National Asphalt Pavement Association.
L.   Oil-fired, production rate of 200 tons/hr during sampling, equipped
     with a cyclone and a baghouse.  "Very little visible emissions from
     stack" observed.  Data provided by the National Asphalt Pavement
     Association.
H.   Oil-fired rotary dryer, production rate varying from 132 to 173 tons/
     hr during sampling, equipped with a cyclone and a  baghouse.   Data
     provided by the National Asphalt Pavement Association.
          Table A-l.  ASPHALT CONCRETE  FACILITY
                     SUMMARY OF RESULTS
Run mmber
1
Date 11/15/71
Test time, minutes
Production rate,
tons/hr
Stack effluent
126
112

How rate, dscfm 16,228
Flow rate, dscf/ton
product
Temperature, "F
Hater vapor, vol .%
C02, vol.* dry
02, vol . % dry
CO, vol.* dry
Visible emissions,
% opacity
8693
195
18.35
0.9
19.2
0
<10
2
11/16/71
63.0
89

16,139
10,880
196
18.38
4.6
14.8
0.1
<10
3
11/17/71
63.0
98

16,520
10,114
187
17.48
4.0
15.4
0.1
<10
Averagi

84.0
99.7

16,296
9896
192.7
18.07
3.2
16.5
0.1
<10
Participate emissions
     Probe and filter catch
gr/dscf
gr/acf
Ib/hr
lb/ ton of
product
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
0.0057
0.0037
0.79
0.007

0.02/2
0.0176
3.78
0.033
0.0077
0.0050
1.06
0.011

0.0194
0.0126
2.68
0.029
0.0068
0.0045
0.98
0.010

0.0184
0.0122
2.60
0.027
0.0067
0.0044
0.94
0.009

0.0217
0.0141
3.02
0.030

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Table A-2.   ASPHALT CONCRETE FACILITY
           SUMMARY OF RESULTS
                                                                                                            Table A-3.  ASPHALT CONCRETE FACILITY B,
                                                                                                                       SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Production rate,
      tqns/hr
Stack effluent
     Flow rate, dscfm
     Flow rate, dscf/ton
                product
     Temperature, °F
     Water vapor, vol.i
     C02. vol.J dry
     02, vol . % dry
     CO, vol .% dry
Visible emissions,
     % opacity
Participate emissions
     Probe and filter catch
          gr/dscf
          gr/acf
          Ib/hr
          Ib/ton of
             product
                  7/20/72
                    12
                  15,650
                   8165

                    218
                   28.2
                    4.5
                   12.8
                    0
                   0.021
                     2.8
                    0.0243
Run number
Date
Test time, minutes
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, °F
Water vapor, vol:%
C02, vol .% dry
0. , vol . % dry
CO, vol .% dry
Visible emissions,
% opacity
Particulate emissions
1
11/11/71
144
203

19,756
5839
275
31.71
5.3
14.1
n.<15
<10

2
11/13/71
90
198

21 ,065
6383
247
23.71
5.8
13.6
0.05
<10

3
11/13/71
90
236

22 ,407
5697
234
21.78
5.1
14.6
0.05
<10

Average

108.0
212.3

21 .076
5973
252
25.73
5.4
14.1
0.05
<10

Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
0.0079
0.0038
1.34
0.007

0.1006
0.0490
17.04
0.089
0.0100
0.0056
1.80
0.012

0.0550
0.0308
9.94
0.066
0.0064
0.0038
1.23
0.005

0.0168
0.0099
3.23
0.014
0.0081
6.0044
'l.46
0.008

0.0575
0.0299
10.07
0.056

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Table A-4.   ASPHALT CONCRETE FACILITY C,



          SUMMARY OF RESULTS
Table A-5.  ASPHALT CONCRETE FACILITY  D,



           SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, °F
Water vapor, vol.3!
C02> vol.* dry
02, vol. % dry
CO, vol .% dry
Visible emissions,
% opacity
Partlculate emissions
1
11/18/71
—
130

36,522
16,856
• 90
2.82"
-

-
--

2
11/18/71
--
130

35,399
16,338
- 90
4.70
--
No
-'-
—

3
11/19/71
--
175

36,148
12,394
-90
4.34
--
4
11/19/71
-
175

34,883
11,960
90
4.51
-
Average


152.5

35,738
14,387
90
4.09
--
orsat available
-
—

—
—


--

Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
0.022
0.019
7.09
0.054

0.024
0.021
7.51
0.058
0.021
0.018
6.68
0.051

0.024
0.020
7.28
0.056
0.012
0.010
3.89
0.022

0.013
0.011
4.03
0.023
0.012
0.010
3.82
0.022

0.013
0.011
3.89
0.022
0.017
0.014
5.37
0.037

0.018
0.016
5.68
0.040
Run nunfcer
Date
Test time, minutes
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, °F
Water vapor, vol.2
C02, vol.* dry
Og, vol. X dry
CO, vol.* dry
Visible emissions,
X opacity
Partlculate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
1b/ ton of
product
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
1
10/29/71
48
221

24,028
6523
238 .
21.6
3.0
14.8
0
<10


0.0122
0.0071
2.49
0.010

0.0517
0.0302
10.64
0.044
2
10/29/71
48
234

23,919
6133
230
23.2
4.6
12.7
0
<10


0.0234
0.0136
4.80
0.020

0.1281
0.0746
26.26
0.109
Average

48
222.5

23,974
6328
234
22.40
3.8
13.8
0
<10


0.0178
0.0104
3.64
0.015

0.0899
0.0524
18.45
0.076
                                                                                                                              11

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         Table  A-6.   ASPHALT CONCRETE  FACILITY  E,
                    SUMMARY  OF RESULTS
Run number 1
Date 11/4/71
Test time, minutes 65
Production rate.
tons/hr
Stack effluent
Flow rate, dscfm 21.706
Flow rate, dscf/ton
product
Temperature, "F 262
Water vapor, vol.% 23.3
CO,, vol .% dry
02, vol. % dry
CO, vol.% dry
Visible emissions,
% opacity
2 Average
11/11/71
65.4 65.2


21,651 21,678
_- --
268 266
27.1 25.2
__ --

"

Participate emissions
     Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
0.0163^
0.0093
3.03
~


0.025
0.0142
4.74
„

0.0215
0.0122
3.99
-


0.029
0.0160
5.47
__

0.0189
0.0108
3.51
--


0.027
0.0151
5.10
—

                                    12
        Table A-7.  ASPHALT CONCRETE FACILITY E,
                   SUMMARY OF RESULTS
Run number
Date
Test. time, minutes
Production rate.
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, °F
Water vapor, vol.%
O>2, vol.% dry
02, vol. % dry
CO, vol .% dry
Visible emissions.
% opacity
1 2
9/25/68 9/26/68
120 120
—


26,160 26,160
„

281 281
24 24
No orsat available
No orsat available
No orsat available
—

Average

120



26,160


281
24



"

Partlculate emissions
     Probe and filter catch
          gr/dscf
          gr/acf
          Ib/hr
                                                                                                                                    Could not be calculated
                                                                                                                                        from test report
Ib/ton of
product
Total catch
gr/dscf °-°06 °-°°7
gr/acf °-003 °-°°4
, ,r 1 57
Ib/hr K35
Ib/ton of
product .



0.0065
0.004
1.46



                                                                                                                                      13

-------
         Table A-8.  ASPHALT CONCRETE  FACILITY G.

                   SUMMARY OF RESULTS8
Run number
Date
Test time, minutes
Production rate,
tons/hr
Stack effluent
. Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, °f
Mater vapor, vol.i
C02, vol.* dry
0, , vol . % dry
CO, vol .« dry
Visible emissions,
% opacity
Participate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
lb/ ton of
product
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
1
7/23/70
60
74

17,092
13,858
107
2.0
No
No
No
--


0.0133
0.0122
1.994
0.027

0.0143
0.0134
0.029
2.137
2
7/23/70
60
	

--
—
-
—
orsat available
orsat available
orsat available
--


0.0162
--
--
--

--
--
—

                                                       Average
                                                          60
Table A-9.   ASPHALT CONCRETE FACILITY  H.,

            SUMMARY OF  RESULTS
                                                         0.01525
'Tested by local agency using Code Method  3.
                                  14
Run number
Date
Test time, minutes
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, °F
Water vapor, vol .%
C02, vol .« dry
02, vol. % dry
CO, vol.? dry
Visible emissions,
% opacity
Paniculate emissions
1
11/4/71
54
176

28,217
9619
112
9.2
3.3
16.6
0.1
--

2
11/4/71
54
193

28,118
8741
109.1
8.4
. 3.1
16.4
0
--

3
11/5/71
54
170

26,126
9221
122
12.2
3.9
15.9
0
~~

Average

54
. 180'

27.487
9194
114
9.93
3.4
16.3
0
."

Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
0.0314
0.0259
7.63
0.043

0.0497
0.0409
12.02
0.068
0.0340
0.0282
8.15
0.042

0.1087
0.0901
26.19
0.136
' 0.0292
0.0229
6.27
0.037

0.0555
0.0435
12.43
0.073
0.0315
0.0257
7.35
0.041

0.0713
0.0582
16.88
0.092
                                                                                                                                15

-------
          Table A-10.  ASPHALT CONCRETE FACILITY
                     SUMMARY OF RESULTS
Run number                     1
tote           =•         .   11/17/71
Test time, minutes            70
Production rate,               200
      tons/hr
Stack effluent     ' '         '.
     Flow rate, ds'cfm  '•     29,400
     Flow rate, dscf/ton      8820
                product
     Temperature, °F          HO
     Water vapor, vol .if       8.7
     CO,, vol.i dry
     0-, vol. % dry
     CO, vol.% dry            --
Visible emissions,
     % opacity
Partlculate emissions
     Probe and filter catch
          gr/dscf            a.Cll
          gr/acf
          Ib/hr
          Ib/ton of
             product
     Total catch
          gr/dscf
          gr/acf
          Ib/hr
          lb/ton of
             product
0.022

5.05
0.025
                                    16
                                                                       Table A-ll.  ASPHALT CONCRETE FACILITY I,
                                                                                  SUMMARY OF RESULTS
                                                             Run number                     1
                                                             Date                        7/17/72
                                                             Test time, minutes
                                                             Production rate,
                                                                   tons/hr
                                                             Stack effluent
                                                                  Flow rate, dscfm       30,460
                                                                  Flow rate, dscf/ton
                                                                             product
                                                                  Temperature, °F         175
                                                                  Water vapor, vol.?        15
                                                                  C02, vol.* dry            --         ,
                                                                  02, vol.'t dry
                                                                  CO, vol.% dry
                                                             Visible emissions,
                                                                  X opacity
                                                             Partfculate emissions
                                                                  Probe and filter catch
                                                                       gr/dscf           0.025
                                                                       gr/acf
                                                                       Ib/hr             6.45
                                                                       Ib/ton of
                                                                          product
Total catch
     gr/dscf
     gr/acf
     Ib/hr
     Ib/ton of
       • product
                                                                                          0.026
6.75

-------
         Table A-12.  ASPHALT CONCRETE  FACILITY J,
                    SUMMARY OF RESULTS
Run number 123
Date (10/16/72 and 10/17/72)
Test time, minutes 80 80 80
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm 17,060 17,060 17,060
Flow rate, dscf/ton
product
Temperature, "F 268 268 268
Water vapor, vol.* 25 25 25
C02, vol.* dry
02, vol. % dry
CO, vol.? dry
Visible emissions,
% opacity
Average

80
"'

17,060

268
25
"



Paniculate emissions
     Probe and filter catch
          gr/dscf          °-°0571
          gr/acf
          Ib/hr             2.89
          Ib/ton of
             product
0.01142    0.01423
1.894
           2.301
                         0.01012
                          2.362
                                    18
                                                                       Table A-13.  ASPHALT CONCRETE FACILITY K,
                                                                                   SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, "F
Water vapor, vol.?
C02> vol.! dry
02> vol. X dry
CO, vol.* dry
Visible emissions,
% opacity
Participate emissions
1
8/22/72
61.25
120

23,000
1 1 ,500
207
14.3
4
15
0
--

2
8/22/72
61.25
120

21 ,700
10,850
205
14.0
4
15
0
—

3
8/22/72
61.25
120

17,800
8900
189
16
4
15
0
—

Averagi

61.25
120

20,500
10,417
200
14.8
4
15
0
—

Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
0.0534
--
10.5
0.0875
0.0918
--
17.1
0.1425
0.180
--
27.5
0.2291
0.108

18.4
0.1530
                                                                                                                                       19

-------
Table A-14.  ASPHALT CONCRETE FACILITY L,
           SUMMARY OF RESULTS
Run number
Date
Test time minutes
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, "F
Water vapor, vol .%
COj, vol.* dry
02> vol . X dry
CO, vol .* dry
Visible emissions,
X opacity
Partlculate emissions
1
8/21/72
60
206

29,900
8970
193
22.3
6
12
0
--

2
8/21/72
60
200

30,700
9210
200
21.0
6
12
0
--

3
8/21/72
60
200

27,200
8160
200
26.7
6
12
0
~~

Average

60
200

29,267
8780
198
23.3
6
12
0
—

Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
0.00447
--
14.1
0.0057
0.00402
--
1.06
0.0053
0.0131
--
3.05
0.0152
0.00720
-
1.75
0.0087
                          20
Table A-15.  ASPHALT CONCRETE FACILITY H,
           SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Production rate,
tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
product
Temperature, °F
Water vapor, vol .%
C02, vol.? dry
02 , vol . % dry
CO, vol .« dry
Visible emissions,
% opacity
Participate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of
product
1
7/14/72
67.5
173

18,290
6345
251
27.1
e
10.6
0
—


0.043
--
6.74
0.0389
2
7/14/72
67.5
132

18,270
8304
245
26.2
8
10.6
0
--


0.043
--
6.73
0.0501
Average

67.5
153

18,280
7325
248
26.7
8
10.6
0
—


0.043
—
6.735
0.0445
                                                                                                                                21

-------
                            PETROLEUM REFINERIES
                        FLUID CATALYTIC CRACKING UNITS
PARTICULATE TEST RESULTS
     Stack tests were carried out at four fluid catalytic cracking
(FCC) units located 1n different petroleum refineries.  At each
Installation, carbon monoxide emissions were controlled by the use
of an Incinerator waste heat boiler (carbon monoxide boiler) and
paniculate matter by the use of an electrostatic precipltator.
Effluent gases were sampled after they had passed through both
control devices.  At one  of the sites tested by EPA, particulate
emissions also were measured by refinery personnel.  Six other
units were tested by a local agency and one by a refinery.

Facilities:
A.   FCC unit of about 55,000-bbl/day capacity, equipped with an
     electrostatic precipltator followed by a carbon monoxide
     boiler.  Tables A-16 and A-17  summarize results of tests
     conducted  in December 1971 and February 1972.  Unit had
     been onstream about six months and eight months,  respectively,
     following  the last major turnaround.  Additional  source  test
     data were  supplied by the refinery  and  are  listed 1n Table A-21.
     These were determined using  Code  Method 6.

 B.   FCC  unit of about 70,000-bbl/day capacity,  equipped with a
     carbon  monoxide  boiler  followed by  an electrostatic  precipltator.
     Unit  had been  onstream  about 10 months  following  the last
                                 22
     major turnaround at the time of the test.  Ammonia was
     injected into the gas stream ahead of the precipltator as a
     conditioning agent.
C.   FCC unit of about 65,000-bbl/day capacity, equipped with a
     carbon monoxide boiler followed by an electrostatic precipltator.
     Unit had been onstream about 13 months following the last
     major turnaround.  Ammonia was Injected into the effluent
     ahead of the precipltator as a conditioning agent.  During
     the test, a malfunction occurred in the FCC unit.

D.   FCC unit of about 55,000-bbl/day capacity, equipped with an
     electrostatic precipitator followed by a carbon monoxide
     boiler.  Unit had been onstream about 8 months following the
     last major turnaround.  During the test, an equipment mal-
     function occurred, Invalidating the particulate results.

E.   FCC unit of about 45,000-bbl/day capacity, equipped with an
     electrostatic precipitator followed by a carbon monoxide
     boiler.  Tested by refinery personnel using Code Method 6
     (alundum thimble packed with glass wool followed by a Gelman
     type A glass fiber filter).  Emission data gathered over
     18-month period of operation.

F.   FCC unit of about 65,000-bbl/day capacity, equipped with a
     carbon monoxide boiler followed by an electrostatic precipltator.
     Tested by local control agency using Code Method 5.
                                                                                                                             23

-------
6.   FCC unit of about 30,000-bbl/day capacity, equipped with an
     electrostatic preclpltator followed by a carbon monoxide
     boiler.  Tested by local control agency using Code Method 5.
H.   FCC unit of 45,000-bbl/day capacity, equipped with an electro-
     static preclpltator followed by a carbon monoxide toller
     Tested by local control agency using Code Method!5.
I.   FCC unit of about 55,000-bbl/day capacity, equipped with an
     electrostatic preclpltator followed by a carbon monoxide boiler.
     Tested by local control agency using Code Method 5.
J.   FCC unit of about 45,000-bbl/day capacity, equipped with a
     carbon monoxide boiler followed by an electrostatic preclpltator.
     Tested by local control agency using Code Method 5.
K.   FCC unit of about 55,000-bbl/day capacity, equipped with an
     electrostatic preclpltator followed by a carton monoxide
     boiler.  Tested by local control agency using Code Method 5.
                                 24
Table A-16.  CATALYTIC CRACKING FACILITY
            SUMMARY OF RESULTS
Run number
Date,
Test time, minutes
Stack effluent
Flow rate, dscfm
Temperature, °F
Mater vapor, vol .
C02, vol . % dry
02, vol. % dry
1
12/16/71
120

185,200
645
. % 17.9
13
4
Carbon monoxide emissions, 14
' ppm (volume)
Visible emissions,
% opacity
Participate emissions
Probe and filter
gr/dscf
gr/acf
Ib/hr
Total catch
gr/dscf
gr/acf
Ib/hr

10


catch
0.1 02T*
0.0410
161. 9a

0.2866a
0.11503
455.6
2
12/17/71
120

175,600
655
19.4
14
4
Nil

10



0.0156
0.0061
23.5

0.0246
0.0096
37.0
3
12/17/71
120

171,100
661
19.7
14
4
Nil

10



0.0114
0.0044
16.7

0.0174
0.0067
25.5
Average

120

177,300
653
19
14
4
5

10



0.0135
0.0053
20.1

0.0210
0.0034
31.2
                                                                                                aExcess1ve emissions.   Test run not considered representative of normal
                                                                                                operation, and not included in averages.
                                                                                                                                    25

-------
Table A-17.  CATALYTIC CRACKING FACILITY
             SUMMARY OF RESULTS
Table A-18.  CATALYTIC CRACKING FACILITY
            SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Stack effluent
Flow rate, dscfm
Temperature, °F
Water vapor, vol.
C02> vol. t dry
02, vol. X dry
1
2/8/72
120 .

183,800
652
X 21.5
11.2
6.4
Carbon monoxide emissions, 10
ppm (volume)
Visible emissions.
% opacity
Partlculate emissions
Probe and filter
gr/dscf
gr/acf
Ib/hr
Total catch
gr/dscf
gr/acf
Ib/hr

10


catch
0.0233
0.0088
36.7

0.0331
0.0125
52.1
2
2/9/72
120

183,900
666
20.9
12.8
4.4
9

10


3
2/10/72
120

184,700
686
22.0
13.2
4.0
11

10


Average

120

184,100
668
21.5
12.4
4.9
10

10


Run number
Date
Test time, minutes
Stack effluent
Flow rate, dscfm
Temperature, °F
Water vapor, vol. %
C02, vol. * dry
02, vol. % dry
Carbon monoxide emissions
ppm (volume)
Visible emissions,
% opacity
Partlculate emissions
1
12/9/71
120

180,600
543
14.5
13.0
3.0
, Nil

30


2
12/9/71
60

183,500
519
15.5
12.0
3.8
Nil

30


3
12/10/71
60

187,000
547
16.9
14.0
3.0
Nil

25


Average

80

183,700
536
15.6
13.0
3.3
Nil

30


Probe and filter catch
0.0202
0.0076
31.8

0.0272
0.0102
42.8
0.0225
0.0082
35.6

0.0308
0.0112
48.7
0.0220
0.0082
34.7

0.0304
0.0113
47.9
gr/dscf
gr/acf
Ib/hr
Total catch
gr/dscf
gr/acf
Ib/hr
0.0355
0.0161
54.2

0.1055
0.0480
162.5
0.0364
0.0166
56.6

0.1320
0.0602
207.6
0.0403
0.0177
64.1

0.1219
0.0534
195.5
0.0374
0.0168
58.3

0.1198
0.0539
188.5
                           26
                                                                                                                                 27

-------
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laoie A-iU. UMALTiii- cnMUPuna rnuiLiiT u,
SUMMARY OF RESULTS


Run number ] 2 3
Date 12/14/71 12/15/71 12/16/71
Test time, minutes 150 240 120


' Stack effluent

How rate, dscfm 196,400 186,400 205,000

Temperature, °F 739 732 723
Mater vapor, vol. X 24.7 23.2 20.6
C02, "vol. % dry 7.0 7.0 10.2
0-, vol. % dry 12.4 12.4 7.4

Carbon monoxide emissions, N11 Nil * N11
ppm (volume)
Visible emissions, 15 10 15
I opacity






























29




4 Average
12/16/71
i on i AO
1 £\t I OU



195,800 195,900

734 732
25.9 23.6
13.1 9.3
3.8 9.0

6 Nil
15 15

































-------
      Table A-21.  ADDITIONAL PARTICULATE EMISSION  DATA
               FOR CATALYTIC CRACKING FACILITIES
Stack Effluent
Facility A.a flow rate, dscfm
	 * 	 3_ 	
Low
High •
Average
Facility Eb
Low
High
Average
Control agency datac
Unit F
Unit G
Unit H
Unit I
Unit J
Uni-t K
166,000
202,000
181,000
106,000
194,000
161,000
169,500
233,300
171,600
224,400
198,300
226 ,900
Concentration
gr/dscf gr/acf
0.010 0.0031
0.021
0.014
0.015
0.022
0.017
0.017
0.018
0.017
0.013
0.020
0.018
0.0067
0.0044
0.0066
0.0094
0.0076
0.0077
0.0059
0.0062
0.0045
0.0085
0.0061
Emission
rate,
Ib/hr
16
34
22
13.6
28.2
23.3
24.7
36.0
25.0
25.0
34.0
35.0
aData covers 7 months operation with  two emission tests per month,
alundum thimble plus glass  fiber  filter (Code  Method 6).
 Data covers 17 months operation  with an emission test about every
2 months, alundum  thimble plus glass  fiber filter (Code Method 6).
cData supplied by  control agency  covering 18 emission tests, Los
Angeles County APCD method  (Code  Method 5).  Impingers precede filter.
                                 30
                      SECONDARY LEAD SMELTERS AND REFINERIES,
                         BLAST AND REVERBERATORY FURNACES
     Test results  are  summarized  for seven blast furnaces and three
reverberatory furnaces.   A local  agency supplied-test data for three
of the blast furnaces  and one reverberatory  furnace.  Nine of the 10
furnaces were equipped with baghouses, six employed afterburners to
bum combustibles, and two units  had scrubbers  for control of sulfur
dioxide.
Facilities:

A.   Blast furnace rated at 77 tons of lead  per day, equipped with
     an afterburner and baghouse.

B.   Two blast furnaces having a  combined rating of 80 tons of lead
     per day, equipped with an afterburner,  baghouse, and venturi
     scrubber, calcium hydroxide  liquor circulated in scrubber.
C.   Blast furnace rated at 45 tons of lead  per day, equipped with
     a caustic venturi scrubber,  sodium hydroxide liquor circulated
     In scrubber.

D.   Blast furnace having an estimated production rate of 90 tons of
     lead per day, equipped with  afterburner and baghouse.  Tested
     by local agency using Code Method 9.

E.   Blast furnace having an estimated production of 20 tons of lead
     per day, equipped with afterburner and  baghouse.  Tested by
     local agency  using Code Method 9.
                                                                                                                        31

-------
F.   .Blast furnace having an estimated production  rate  of 52 tons

     of lead per day,  equipped with afterburner and baghouse.  Tested

     by local  agency using Code Method 9.


6.   Reverberatory furnace rated at 40 tons of lead per day  equipped

     with baghouse.


H.   Reverberatory furnace rated at 65 tons of  lead per day, equipped

     with baghouse.


I.   Reverberatory furnace having  an  estimated  production of 20  tons

     of lead per day, equipped with a baghouse.   Tested by  local

     agency  using Code Method 9.
                                   32
Table A-22.  LEAD SMELTING FACILITY A,

         SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Lead production, tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
Temperature, °F
Water vapor, vol . %
COj, vol . % dry
Oj>, vol. I dry
CO emissions, vol. 4 dry
CO emissions, Ib/hr
SOj emissions, ppm dry
S02 emissions, Ib/hr
Visible emissions.
% opacity
1
11/17/71
91
3.7

23,200
376,200
176
3.7
2.2
19.0
0.5
503
443
701
10 to 15

2
11/18/71
188.
2.5

22,900
549,600
182
:2.3
2.1
19.0
0.2
199
264
59
10 to 70

3
11/18/71
186
3.0s

23,120
462,400
177
3.1
1.5
19.5
0.4
401
204
46
5 to 15

Average

155
3.T

'23,070
462,700
178
3.0
1.9
19.2
0.36
368
304
69
12

                                                                                               Participate emissions

                                                                                                    Probe and filter  catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
0.0028
0.0022
0.5541
0.1498

—
0.0027
0.0021
0.5231
0.2092

0.0471
0.0368
9.2439
3.6976
0.0023
0.0018
0.4570
0.1523

0.0396
0.0310
7.8566
2.6189
0.0026
0.0020
0.5114
0.1704

0.0434
0.033?
8.5503
3.1583
                                                                                               Lead emissions

                                                                                                   Probe and filter catch

                                                                                                        gr/dscf
                                                                                                        gr/acf
                                                                                                        Ib/hr
                                                                                                        Ib/ton lead

                                                                                                   Total catch
                       0.00035
                       0.00027
                       0.0679
                       0.0272
0.00033
0.00026
0.0648
0.0216
0.00034
0.00027
0.0664
0.0244
                                                                                                                               Essentially the  same as probe and filter.
                                                                                               aThe lead holding pot level was altered by plant personnel during this test
                                                                                                and a rate based on average  production figures  was assumed.
                                                                                                                                33

-------
                      Table A-23.   LEAD SMELTING FACILITY  B,
Run number

Date
SUMMARY OF  RESULTS

     1           2          3


 12/15/71     12/16/71    12/16/71
Visible emissions, % opacity

Partlculate emissions

     Probe  and filter catch

         gr/dscf
         gr/acf
         Ib/hr
         Ib/ton lead

     Total  catch

         gr/dscf
         gr/acf
         Ib/hr
         Ib/ton lead

Lead emissions

     Probe  and filter catch

         gr/dscf
         gr/acf
         Ib/hr
         Ib/ton lead

     Total  catch
                                                                   Average
Test time, minutes
Lead production, tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
Temperature, °F
Hater vapor, vol . %
C02 , vol . % dry
Oj, vol . t dry
CO emissions, vol. % dry
CO emissions, Ib/hr
502 emissions, ppm dry
S02 emissions, Ib/hr
S02 Inlet, pom dry
SOj Inlet, Ib/hr
195
4.2

32,060
458,000
124
6.34
3.2
16.8
<0.1
139
1050
334
1680a
534
200
4.9

29,420
360,200
121
10.33
2.8
17.0
0.2
255
310
90
1100
321
200
3.5

38,060
652,500
118
11.04
3.4
16.4
0.4
660
138
52
1900b
718
198
4.2

32,960
490,200
121
9.24
3.1
16.7
0.23
350
499
159
1560
524
0.0079
0.0066
2.1743
0.5177
0.0417
0.0348
11.4461
2.7253
0.00011
0.00009
0.0300
0.0070
0.0042
0.0033
1.0551
0.2153
0.0364
0.0290
9.1715
1.8717 -
0.00013
0.00010
0.0328
0.0067
0.0115
0.0094
3.7600
1.0713
0.0454
0.0372
14.8245
. 4.2356
0.00016
0.00013
0.0506
0.0145
0.0079
0.0064
2.3298
0.6024
0.0412
0.0366
11.8140
2.9442
0.00013
0.00011
0.0378
0.0094
                                  Essentially the  same as probe and filter.
 "Scrubber pH add for portions of test (control  efficient lowered).
  Scrubber operating properly.
   34
                                                                                                                            Table  A-24.   LEAD SMELTING FACILITY C,
                                                                                                                                     SUMMARY OF RESULTS
Run number

Date

Test time, minutes

Lead production,  tons/hr

Stack effluent

     Flow rate, dscfm
     Flow rate, dscf/ton
     Temperature, °F
     Water vapor, vol. %
     C02, vol. % dry
     02, vol. % dry
     CO emissions, vol. X dry
     CO emissions, Ib/hr
     SOj emissions, ppm dry
     SOj emissions, Ib/hr

Visible emissions,
     i opacity

Partfculate emissions

     Probe and filter catch

          gr/dscf
          gr/acf
          Ib/hr
          Ib/ton lead

     Total catch

          gr/dscf
          gr/acf
          Ib/hr
          Ib/ton lead

Lead emissions

     Probe and filter catch

          gr/dscf
          gr/acf
          Ib/hr
          Ib/ton lead

     Total catch
1
12/8/71
120
1.5
12,100
484,000
97
2.4
0.5
20.3
0.8
420
0.06
0.01
2
12/9/71
112
1.2
13,330
666,500
95
1.7
0.8
20.2
0.3
160
0.04
0.01
3
12/9/71
112
1.2
12,540
627,000
93
2.3
0.8
18.8
0.2
109
0.08
0.01
Average

115
1.3
12,657
592,500
95
2.13
0.7
19.7
0.4
330
0.06
0.01
                                                                                                                                      10 to 15    10 to 20    5 to 15
                                                                                                                                                                            12
0.0196
0.0184
2.0354
1.3570
0.0275
0.0257
2.8474
1.8983
0.00127
0.00119
0.1320
0.0880
0.0084
0.0080
0.8913
0.7750
0.0157
0.0149
1.6556
1.4397
0.00061
0.00058
0.0646
0.0562
0.0149
0.0140
1.6061
1.2849
0.0235
0.0221
2.5200
2.0160
0.00127
0.00120
0.1368
0.1095
0.0143
0.0135
1.5109
1.1389
0.022r
0.0208
2.3410
1.7847
0.00105
0.00099
0.1111
0.0846
                                                                                                                                         Essentially the same as probe and filter
                                                                                                                                       35

-------
                       Table  A-25.   LEAD  SMELTING FACILITY D,

                                SUMMARY OF  RESULTS3
Lead production,  tons/hr

Stack effluent          „  ,. .

     Flow rate, dscfm
     Flow rate, dscf/ton
     Temperature, °F
     Water vapor, vol.  %
     •C02, vol. % dry
     02, vol.  I dry
     CO emissions, vol. X dry
     CO emissions, Ib/hr
     S02 emissions, ppm dry
     S02 emissions, Ib/hr

Visible emissions, X opacity

Participate emissions

     Probe and filter catch

          gr/dscf
          gr/acf
          Ib/hr
          Ib/ton lead

     Total catch

          gr/dscf
          gr/acf
          Ib/hr
          Ib/ton lead

Lead emissions

     Probe and filter catch

          gr/dscf
          gr/acf
          Ib/hr
          Ib/ton lead
   3.9 (estimated)
 20,900
321,500
   152
   8.7
   4.2
 .16.8
   1.5
  1363
  1170
   248
 0.0013
 0.0010
 0.233
 0.060
 0.0075
 0.0059
 1.344
 0.345
  0.00061
  0.00048
  0.1093
  0.0280
  Tested by local  agency using  Code Method  9.
                                    36
                                                                                     Table A-26.  LEAD SMELTING  FACILITY  E,

                                                                                                SUMMARY OF  RESULTS3
Lead production, tons/hr
•Stack effluent
•• • £ ;
Flow rate, dscfm
.Flow rate, dscf/ton • -
Temperature, °F . •_
Hater vapor, vol. %
S02 emissions, ppm dry
S02 emissions, Ib/hr
Visible emissions, % opacity
Participate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
0.8 I


; 13,000
975,000
175
3.9
300
40
0


0.0059
0.0047
0.657
0.822

0.0350
0.0281
3.900
4.875
                                                                                                          Tested by local  agency using Code Method 9.
                                                                                                                                             37

-------
Lead production, tons/hr
Stack effluent
     FTow rate, dscfm
     Flow rate, dscf/ton
     Temperature, °F
Visible emissions, % opacity
Participate emissions
     Probe and filter catch
          gr/dscf
          Ib/hr
          Ib/ton lead
     Total  catch
          gr/dscf
          Ib/hr
          Ib/ton lead
Table A-27.  LEAD SMELTING FACILITY F,
          SUMMARY OF RESULTS3   .
                     2.2 (estimated)
                   .7500
                  204,500
                     110
                  10 to 30
                   0.0142
                   0.913
                   0.415

                   0.084
                   5.400
                   2.455
"Tested by local agency using Code Method 9. ,
                                  38
                           '-:>    •:«
                           :.ac   '-.
                           "?i.
                                                                                                                                  Table A-28.   LEAD SMELTING  FACILITY G,
                                                                                                                                            SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Lead production, tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
Temperature, °F
Water vapor, vol. %
C0£ , vol . % dry
02, vol. I dry
CO emissions, volj. % dry
CO emissions, Ib/hr
SO- emissions, ppm dry
S02 emissions, Ib/hr
Visible emissions, % opacity
Paniculate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Lead emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
1
1/26/72
120
2.1

14,600
417,100
166.
3.1
1.8
18.6
<0.1
63.5 '
1580
229
0


0.0043
0.0035
0.5387
0.2565

0.0132
0.0170
1.6520
0.7867


0.00090
0.00073
0.1130
0.0538

0.0010
0.00081
0.1262
0.0601
2
1/26/72
. 120
.2.1

15,200
434,300
164
2.8
1.8
18.7
<0.1
66.0
1525
230
0


0.0028
0.0023
0.3702
0.1763

0.0086 .
0.0070
1.1148
0.5309


0.00049
0.00040
0.0640
0.0305

—
. —
—
—
3
1/26/72
120
2.1

14,200
405,700
175
3.1
1.8
18.7
<0.1
61.7
1618
228
0


0.0035
0.0028
0.4297
0.2046

0.0200
0.0161
2.4321
1.1581


0.00045
0.00037
0.0553
0.0263

	
—
--
—
Average

120
2.1

14,667
419,000
168
3.0
1.8
18.7
<0.1
63.7
1574
229
0


0.0035
0.0029
0.4462
0.2125

0.0139
0.0113
1.7330
0.8252


0.00061
0.00050
0.0775
0.0369

0.00100
0.00081
0.1262
0.0601
                                                                                                                                                 39

-------
Table A-29. LEAD SMELTING FACILITY H,
SUMMARY OF RESULTS
Run number
Date

Test time, minutes
Lead production, tons/hr
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
Temperature, °F
Water vapor , vol . %
C02 , vol . I dry
Oj. vol. % dry
CO emissions, vol. % dry
CO emissions, Ib/hr
SO* emissions, ppm dry
S0| emissions, Ib/hr
Visible emissions. % opacity
Partlculste emissions
Prcoe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Lead emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton lead
1
2/9/72
i
150
2.4

23,480
587,000
124
4.0
2.4
18.2
<0.1
<102
2060
480
0


0.0024
0.0021
0.4890
0.2038

~ 0.0118
0.0100
2.3737
0.9890


0.00034
0.00029
0.0692
0.0288

0.00050
0.00043
0.1035
0.0432
2
2/9/72

150
2.4

22,600
565,000
132
4.6
2.5
18.0
<0.1
<98
2111
473
0


0.0033
0.0027
0.6350
0.2646

0.0131
0.0109
2.5398
1.0583


0.00039
0.00033
0.0763
0.0318

__
—
	
~
3
2/10/72

150
2.4

19,940
498,500 .
117
4.2
2.0
. 18.2
<0.1
<87
1930
381
0


0.0042
0.0036
0.7205
0.3002

0.0164
0.0140
2.7950
1.1646


0.00041
0.00035
0.0695
0.0289

	
	
„
—
Average


150
2.4

22,007
550,200
124
4.3
2.3
18.1
<0.1
<96
2034
445
: °


0.0033
0.0028
0.6148
0.2562

0.0138
0.0860
2.5695
1.071


0.00038
0.00032
0.0717
0.0298

0.00050
0.00043
0.1035
0.0432
                                                                                          Table A-30.  LEAD SMELTING FACILITY I,
                                                                                                    SUMMARY OF RESULTS"
                                                                     Lead production,  tons/hr
                                                                     Stack effluent
                                                                          Flow  rate, dscfm
                                                                          Flow  rate, dscf/ton
                                                                          Temperature, °F
                                                                          SOj emissions, ppm dry
                                                                          SOj emissions, Ib/hr
                                                                     Visible emissions, %  opacity
                                                                     Partlculate emissions
                                                                          Probe and filter catch
                                                                               gr/dscf
                                                                               Ib/hr
                                                                               Ib/ton  lead
                                                                          Total catch
                                                                               gr/dscf
                                                                               Ib/hr
                                                                               Ib/ton  lead
  0.85 (estimated)

 10,400
734,100
   327
  1039
   110
    0
 0.0022
 0.196
 0.231

 0.0130
 1.159
 1.363
                                                                     aTested by local agency using Code Method 9.
40
                                                                                                         41

-------
                      SECONDARY BRASS AND BRONZE REFINING

     The data summarized herein cover 13  brass and bronze Ingot
production furnaces at 9 different test sites.  Tests AI. B, and
D were conducted  by EPA and EPA contractors.  Tests C, E, F, and
I were conducted  as part of a 1968 study  performed jointly by the
Brass and Bronze  Ingot Institute and the  National Air Pollution
Control Administration, an EPA predecessor.   Tests AZ> G, and H
were conducted  by local control agencies.

Facilities:
A.   Gas-fired  rotary (rotating reverberatory) furnace, 7.5-ton
     capacity,  equipped with two closed suction-type manually
     cleaned baghouses with a total cloth area of 7181 square
     feet.  Tested by EPA and by local agency, the latter using
     Code Method  10.
B.   Gas-fired  reverberatory (stationary  reverberatory) furnace,
     100-ton capacity, equipped with a closed suction-type cyclic-
     cleaned baghouse with a cloth-area of 9000 square feet.
C.   Gas-fired  reverberatory furnace, 60-ton capacity, equipped
     with a closed suction-type cyclic-cleaned baghouse with a
     cloth area of 5940 square feet.  Testing using Code Method
E.   Gas-fired reverberatory furnace, 100-ton  capacity, equipped with a
     closed suction-type cyclic-cleaned baghouse with a cloth area of
     7360 square  feet.   Tested using Code Method 4.
F.   Gas-fired rotary  furnace, 17.5-ton capacity, equipped with a
     closed suction-type cyclic-cleaned baghouse with a cloth area
     of 20,866 square  feet.   Tested using Code Method 4.

G.   Two rotary furnaces with a total capacity of 55 tons, equipped
     with two closed suction-type baghouses with a total cloth area
     of 41,700 square  feet.   Probe and filter  catch were not analyzed
     separately.

H.   Two rotary furnaces with a total capacity of 27.5 tons, equipped
     with three closed suction-type baghouses  with a total cloth area
     of 9536 square  feet.   Probe and filter catch were not analyzed
     separately.

I.   One 7.5-ton  rotary furnace, one 17.5-ton  rotary furnace, and one
     blast furnace,  which was being preheated.   All  three furnaces were
     ducted to a  closed suction-type cyclic-cleaned baghouse with a
     cloth area of 20,866 square feet.  Tested using Code Method 4.
     Oil-fired rotary furnace, 20-ton capacity,  equipped with a
     closed pressure-type cyclic-cleaned baghouse with a cloth
     area of 18,661  square feet.
                                  42
                                                                                                                              43

-------
                           Table A-31.

        Run muter
        Date
       "Test time, minute:
        Heat time, minutes
       -Ingots produced per heat."tons
        Zinc -In alloy produced. .J
        Stack effluent
            Flow rate,^scfa
          -v'Temperatut*. *F
            Hater *apor. Hobe andH'llter^xatch
                 gr/ascf
                 gr/acf-
                 Ib/hr
                 Ib/ton of product
            .Total catch
                - gr/dscf
                 gr/acf
                 Ib/hr
                 Ib/ton of product
BRASS AND
BRONZE FACILITY A,,
JWNARY OF RESULTS
1
11/10/71
582
938
;e:66
-40
13-^539
--84.9 :
3.303
OS
18.4
Nil
0.'002
0.001
0.165
t>.388
-0.0047
. -0.0043
0.521
1.22
.. 2
n/io-n/71
. 771
922
-;-7:80
-37
13.^0 :
-:103.*
3.227 :
: l.o :
16.8
mi
0.0005
0.0005
0.065
0:1 27
0.0011
'0:0010
0.129
0.25
3
11/12/71
733 .
912
7:21
•:gD
. 13^75
.'106.2
3.139
.073
17^4
Nil
0.0003
0.0002
0.010
•0.066
-.0.0016
.0.0014
0.185
0.37
Average

£95
924
7.22
..39.
13^568
- .98.2
'.3.2?3
— r fc«
-: ,^7,3.
H11
;o.ooi.
0.0006
0.080
0.194
0.0024
.0.0022
0.278
0.61
  Run number                  .   -
  Date .
  Z1nc In alloy produced. I (approx.)
.Stack-effluent
      Flow  rats.,dscfm
    -  Teaperature. *T      .
 Partlculate emissions
      Total «^trh
        . -gr/dscf
         ' Ib/nr  .
Table A-32.  BRASS AND BRONZE FACILITY
     .   . SUMMARY OF-RESULTS9
                         1
                      5/11/71
                        40
                      15.468
                        O25
                      0.0023
                      0.286
 tested by local  agency-using .Code-Method .10.  Profaevand-fllier urtdi
.-„ not, analyzed separately.
                                        44
                                                                                                                                       45
|g^j**.  ?^^:;. •:-  ^   ;.. ••.-  ;c\-i;-^v^^-/!^^^ir2«?^^^                                              ^J^^^^^a,;
"r^^-^r-  •±^i^^^'r_-2:_^:'--L:i.i"-''^'"i-'^

-------
Table A-33.   BRASS AND BRONZE FACILITY B,
           SUMMARY OF RESULTS
Table A-34.  BRASS AND  BRONZE FACILITIES C, E, arid F,
                 SUMMARY  OF RESULTS3



























V
I
i

T
*i
Run number
Date
Test time, minutes
Heat time, minutes
Ingots produced per
heat, tons

Z1nc In alloy produced.
t

Stack effluent
Flow rate, dscfm
Temperature, °F
Water vapor, vol. t
C02. vol. t try
0_, vol. t dry
z" *
Excess air at
sampling point, %
Visible emissions,
t opacity
Partlculate emissions
Probe and filter catch

gr/dscf
gr/acf

Ib/hr
*
'• .Ib/ton of product
? Total catch
.; gr/dscf
; gr/ac*
Ib/hr-
. •• Ib/ton of product
1
11/1/71
120
1140
49.09


9



27,515
118
2.66
0.60
19.50

1112

<10




0.006
0.005

1.55
0.60
-
0.022
0.019
5.081
1.98
2
11/2-3/71
700
1183
59.86


5



30,124
107
1.86
0.58
19.58

1117

<10




0.005
0.005

1.25
0.41

0.007
0.006
1.692
0.51
3
11/3-4/71
747
1326
56.36


5



25,406
106
1.85
0.60
19.60

1205

<10




0.007
0.006

1.46
0.43 .

0.008
0.008
1.789
0.68
4
11/4-5/71
780
1372
53.93


5



27,114
113
1.75
0.53
19.60

1210

<1Q




0.004
0.004

0.99
0.42

0.006
0.005
1.356
0.51
Average

656
1255
54.81


6



27,540
111
2,03
0.58
19.57

1176

<10




0.006
0.005

1.31 .
0.46 .

•0.011 .
0.009 ,
2.479 .
0.92
Installation
Run number
Date
Test time, minutes
Heat time, minutes

Metal charged per
heat, tons

Z1nc 1n alloy
produced, %
Stack effluent
Flow rate, dscfm
Temperature, °F
Water vapor, vol. %
CO?, vol . t try
02, vol. % try

Excess air at
sampling point, %
Visible emissions, * opacity

Participate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton charged
Total catch

gr/dscf
gr/acf
Ib/hr
• Ib/ton charged"

aTested using Code Method 4.
C
1
10/22-23/68
~
1326

72


9


18,052
4.51
0.57
19.0


791.0
—



0.013
--
1.93
0.59


0.014
' 2.17
0.67


Tons of scrap charged was used for these
rates were unavailable.


E
1
7/9-10/68
1175
1174

52.7


5


27,049
160
5.0
0.89
17.9


484.0
<10



0.014
--
3.16
1.17


0.014
3.32
1.23


calculations since

F
1
7/7-8/68
879
874

16.7


5


33,999
150
2.6
0.63
18.2


535.0
<10



0.005
__
-1.61
1.41


0.006
1.78
1.56


Ingot production

               46
                                                                                                                        47

-------
Table A-35.  BRASS AND BRONZE FACILITY D,

           SLBMARY OF RESULTS  •
Sun miter
Bate
-•Test tlie* dilutes
Heat tine. minutes
Ingots produced per
••heat, tons
* 21 nc In jTlflj' produced.
I
SUck-effluent
Flow rate, dscfm
'Temperature, -T
Hater vapor. -vol. %
CO., vol . I dry
z
02, vol;:Xdry
. Excess »1r at
.sampling' point. X " "'
Visible emissions.
X opacity
• Paniculate .emissions
Probe anaTllter-catch
.gr/dscf
gr/acf
Ib/hr
•.lb/ton of product
Total catch
gr/dscf
gr/acf
Ib/hr
•lb/ton of product

1
31/30/71
_266
. .534
-18:03

31


28,582
W4
1.250
0.300
20.30
- .2474
- art1 cul ate-esrt sstom
'Total ratch
5r/dscf
=1b/nr
3 2
7/15/70 8/20/70
*0 •<. 9"

-..-52.900 • 52,900
~ 250 ' -250 .


,0.015 - O.fliS - •
-B^BO B^2 '
Average

"75

.,-52,900
250.


• B.017
' J.71
                                                                                           'Conducted by local agency.  Probe and filter catch not analysed
                                                                                            separately.
                                                                                                                              49

-------
                      Table A-37.  BRASS AND BRONZE FACILITY H,
                         .  '  .    SUMMARY OF RESULTS4
                                                              5        6
Run number
Date
Test time, minutes
Stack effluent
Flow rate, dscfra
Temperature, °F
Paniculate emissions
Total catch
gr/dscf
Ib/hr
.1
8/17/70
60

8000
155


0.009
0.62
2
8/17/70
60

8000
155


0.015
1.02
3
3/11/71
60

4100
--


0.019
0.67
4
3/1 2/',
60

4100
-


0.001
0.04
                                                             60
                                                                      60
                                                                               Average
                                                                                 60
                                                           0.016    0.012
Conducted by local  agency.  Probe and filter catch not analyzed separately.
                                                                               0.012
                                       SO
Table A-38.  BRASS AND BRONZE  FACILITY I.
           SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Stack effluent
Flow rate, dscfm
Temperature, °F
Water vapor, vol. %
C02, vol. « dry
02, vol. % dry
CO. vol . % dry
Part icul ate emissions
Probe and filter catch
gr/dscf
Ib/hr
Total catch
gr/dscf
Ib/hr
1
7/8/68
60

33,926
215
4.5
0.65
17.0
Nil


0.012
3.49

0.018
5.18
2
7/8/68
60

33,807
215
3.1
0.63
17.0
Nil


0.007
2.04

0.011
3.32
3
7/9/68
60

36,121
175
3.2
1.43
17.5
Nil


0.010
3.21

0.021
6.39
Averagf

60

34,618
202
3.6
9.03
17.2
N11


0.010
2.91

0.017
4.96
                                                                                                                                                51

-------
                              IRON AND STEEL MILLS
                          BASIC OXYGEN PROCESS FURNACES

     Six emission tests were performed by EPA and EPA contractors on
six basic oxygen process furnace (BOPF) facilities.   The particulate
control systems included two electrostatirc,orecipitator systems, one
open-hood venturi scrubber system, and two movable closed-hood venturi
scrubber systems.  Closed-hood Facility A was tested in November 1971
and again in February 1972.   There were no visible emissions from any
of the plants tested except Facility D.

     Each facility consists of two or three BOPFs.  Normally, two
furnaces are operated at any one time, with the third undergoing
routine rebricking and maintenance.  Each test consisted of four or
six cycles of the furnaces.   Testing was initiated immediately after
the furnace was charged and discontinued just prior to tapping.  Only
one furnace was blown with oxygen during any cycle.

Facilities:

A.  Rated capacity each vessel—220 tons of steel per heat, equipped
    with a closed-hood venturi scrubber system.

B.  Rated capacity each vessel—200 tons of steel per heat, equipped
    with a closed-hood venturi scrubber system.

C.  Rated capacity each vessel—140 tons of steel per heat, equipped
    with an open hood ducted to a cannon electrostatic precipitator.
                                 52
D.   Rated capacity each vessel—325 tons of steel per heat, each
    vess.el equipped with an open hood ducted to a common venturi
    scrubber system.  Oil is burned in the hood between oxygen
    blows to give a constant steam supply.     * '•

E.   Rated capacity each vessel—250 tons of steel per heat, equipped
    with an open hood ducted to a common electrostatic precipitator.
                                                                                                                                               53

-------
           TaSrte A-39.  BOPF FACILITY A, ,

                 SUMMARY OF RESULTS
Run number
Date x
Test time, minutes
Net output (six heats).
tons of steel
Stack effluent
Flow rate, dscfm
Flow rate, dscf/
ton steel
Temperature, "F
Water vapor, vol. %
C02, vol . % dry
02, vol . % dry
CO, vol . % drya
Visible emissions.
% opacity
Participate emissions
1
1/26/72
173
1381.0


58,600
7341

123
13.4



0


2
1/27/72
154
1372.5


55,600
6239

125
13.6
Orsat not
Orsat not
Orsat not
0


3
1/27/72
156
1361.2


58,600
6716

129
12.6
run
run
run
0


Average

161
1371.6


57 ,600
6765

126
13.2



0


Probe and filter catch
gr/dscf
gr/acf
Ib/ton of steel
Total catch
gr/dscf
gr/acf
0.002
0.002
0.0021

0.005
0.004
Ib/ton of steel 0.0048
0.002
0.001
0.0015

0.004
0.003
0.0034
0.005
0.004
0.0048

0.006
0.005
0.0061
0.003
0.002
0.0028

0.005
0.004
0.0047
aStack gases analyzed at point downstream  of  scrubber but upstream of flare.
                                   54


Run number
Date
Test tine, minutes
Net output (six heats),
tons of steel
Stack effluent
Flow rate, dscfm
Flow rate, dscf/
ton steel
Temperature, °F
Water vapor, vol. %
C02, vol. % dry
0- , vol . % dry
CO, vol. % dry3
Visible emissions,
% opacity
Particulate emissions
Table A-40.
SUMMARY
1
11/16/71
162
1331.0

58,880
7166
119
12.9
13.0
8.0
27.0
0 '

BOPF FACILITY
OF RESULTS
2
11/16-17/71
149
1321.3

57,808
6519
117
12.9
19.2
7.3
22.0
0

V

3
11/18/71
168
1298.5

59,621
7714
125
9.8
20.8
7.6
19.0
0



Average

160
1316.9

58,769
7133
120
11.9
17.7
7.6
22.7
0

Probe and filter catch
gr/dscf
gr/acf
Ib/ton of steel
Total catch
gr/dscf -
gr/acf
Ib/ton of steel
0.002
0.002
0.0020

0.005
0.004
0.0052
0.009
0.007
0.0083

0.014
0.011
0.0135
0.003
0.002
0.0031

0.005
0.004
0.0052
0.005
0.004
0.0044

0.004
0.006
0.0039
aStack gases analyzed at point downstream of scrubber but upstream of
 flare.
                                                                                                                                   55

-------


Run number
Date
Test time, minutes
Net output (six heats),
tons of steel
Stack effluent
Flow rate, dscfm
Flow rate, dscf/
ton steel
Temperature, °F
Hater vapor, vol. %
C02, vol. % dry
02, vol . % dry
CO, vol . % dry8
Visible emissions,
% opacity
Table A-41.
SUMMARY
1
10/20/71 '
222
1214.3

37,154
6792
154
10.5
10.4
8.7
27.2
0
BOPF FACILITY B,
OF RESULTS
2
10/21/71
255
1202.7

32,020
6788
161
12.7
9.4
9.7
25.2
0

3
10/23/71
224
1223.8

48,787
8930
128
13.4
10.8
7.5
36.7
0

Average

234
1213.6

39,300
7503
148
12.2
10.2
8.6
29.7
0
Participate emissions
     Probe and filter  catch
         "gr/dscf
          gr/acf
          Ib/ton of steel
     Total  catch
          gr/dscf
          gr/acf
          Ib/ton of steel
0.012
0.009
0.0116
0.014--
0.011
0.0141

0.016
0.012
0.0159
 0.011
 0.009
 0.0141

 0.012
.0.010
 0.0158
0.012
0.010
0.0133

0.014
0.011
0.0158
aStack gases analyzed at point downstream of scrubber but upstream of
 flare.
''The impinger catch of Run 1 was contaminated with stopcock grease.
                                   56
, — r ,

Run number
Date
Test time, rrfnutes
Net output {four heats),
tons of steel
Stack effluent
Flow rate, dscfm
Flow rate, dscf/
ton steel
Tempe--:.-re, °F
Water vapor, vol . %
C02, vol. I dry
02 , vol . % dry
CO, vol . % dry
Visible emissions,
% opacity
Paniculate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/ton of steel
Total catch
gr/dscf
gr/acf
Ib/ton of steel
Table A-42.
SUMMARY
1
11/10/71
141 .'
569.2 '

219,120
54,279
238
14.6
6.2
16.6
<1
0


0.009
0.006
0.0730

0.014
0.009
0.1070
BOPF FACILITY
OF RESULTS
2
11/10/71
143
601.5

215,571
53,042
246
14.8
1.8
19.2
<1
0


0.005
0.003
0.0370

0.008
0.005
0.0631
c,

3
11/11/71
i4
586.0

201 ,071
56,272
234
15.0
5.1
17.4
<1
0


0.006
0.004"
0.0471

0.010
0.006
0.0779


Average

151
585.6

211,921
54,531
238
14.8-
4.4
17.7
<1
0


-0.007
0.004
0.0524

0.011
0.007
0.0826
                                                                                                                                             57

-------
Table A-43. BOPF FACILITY
SUMMARY OF RESULTS ...... nu «,- m-cm TC
D,
Table A-44.
BOPF FACILITY
E,

awuinni u, r,,.ju.- SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Net output (four heats),
tons of steel
Stack effluent
Flow rate, dscfm
Flow rate, dscf/
ton steel
Temperature, °F
Water vapor, vol. %
C02, vol. * dry
02, vol. % dry
CO, vol . % dry
Visible emissions,
% opacity
Particulate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/ton of steel

Total catch
gr/dscf
gr/acf
Ib/ton of steel
1
12/8-9/71
130
1376.6

224,900
21 ,239

134
16.2
1.2
19.3
<1
0 to 20



0.035
0.026
0.106


0.042
0.031
0.1270
2
12/10/71
126
1357.2

217,982
20,237

144
15.4
1.0
19.9
<1
0 to 20



a
-
—


0.040
0.029
0.1160
3
12/10/71
158
1368.1

214,100
24,726

137
12.6
1.0
19.9
<1
0 to 20



a
-
--


0.028
0.021
0.0996
Average

138
1367.3

218,994
22,067

138
14.7
1.1
19.7
<1
0 to 20



-
-
-


0.0368
0.027
0.1142
Run number
Date
Test tine, minutes
Net output (four heats),
tons of steel
Stack effluent
Flow rate, dscfm
Flow rate, dscf/
ton steel
Temperature, °F
Water vapor, vol . *
C02, vol . t dry
0., vol . t dry
CO, vol . t dry
Visible emissions.
% opacity
Particulate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/ton of steel
Total catch

gr/dscf
gr/acf
Ib/ton of steel
1
1/12/72
122
1101.5

522,332
57,852

198
16.0
4.3
17.6
<1
0



0.020
0.014
0.169


0.029
0.020
0.244
2
1/12-13/72
121
1102.9

496,657
54,486

196
19.1
4.9
16.7
<1
0



0.045
0.030
0.352


0.052
0.034
0.402
3
1/13-14/72
115
1087.9

461 .571
48,792

206
20.8
4.9
16.7
<1
0



0.016
0.010
0.109


0.023
0.015
0.161
Average

: 119
1097.4

493,920
53,742

200
18.6
4.7
17.0
<1
• o



0.027
0.018
0.210


0.035
0.023
0.269
aThe filter In Runs 2 and 3 leaked, and it 1s impossible to separate the
 front half catch from the total catch for these runs.
                                   58
                                                                                                                                         59

-------
                           SEWAGE TREATMENT PLANTS
                         SEWAGE SLUDGE  INCINERATORS

     Stack tests were conducted on five sludge incinerators including
three multiple hearth units and two fluid  bed reactors.  One installation
was tested both by EPA and a State agency.  Four of the incinerators
were controlled by impingement-type scrubbers, one was controlled by a
venturi scrubber.  Pressure drops across the scrubbers ranged from
2.5 to 18 inches of water.

Facilities:
A.  Fluidized bed reactor, 1100-lb/hr dry  solids design capacity, _
    operated at 100 percent capacity during test, equipped with a
    20-inch-of-water pressure-drop venturi scrubber operated at
    18 inches water pressure drop.  Tested by EPA and by a State
    agency, latter using Code Method 8.
B.  Multiple hearth (six hearths) Herreshoff incinerator, 750-lb/hr
    dry solids design capacity, operated at 64 percent capacity
    during.test, equipped _with_a_6_.0jrichj-of-water-pressure-drop
    single-cross-flow perforated-plate  inpinjet scrubber.

C.  Multiple hearth (six hearths) Herreshoff incinerator, 900-lb/hr
    dry solids design capacity, operated at 35 percent capacity
    during test, equipped with a 6.0-inch-water-pressure-drop
    single-cross-flow perforated-plate  impinjet scrubber.

D.  Fluidized bed reactor, 500-1b/hr dry sol Ids design capacity, operated
    at 95 percent capacity during test, equipped with a 4.0-inch-water-
    pressure-drop single-cross-flow perforated-plate Impinjet scrubber.
                                  60
E.  Multiple  hearth Herreshoff  incinerator, 2500-lb/hr  dry solids
    design'capacity, operated at  about 50 percent  capacity during
 •   tests,  equipped with a  2.5-inch-water-pressure-drop cyclonic
    inertial  jet scrubber.
                                                                                                                                                 61

-------
         Table A-45.  SLUDGE INCINERATOR FACILITY A,,

                     SUN4ARY OF RESULTS
                                                                                                                Table A-46.  SLUDGE INCINERATOR FACILITY A2>
Run number
Date
Test time, minutes
Furnace feed rate.
ton/hr dry solids
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
feed '
Temperature, °F
Hater vapor, vol. *
C02, vol. % dry
Oj , vol . X dry
CO, vol. % dry
S02 emissions, ppm
NO, emissions, ppm
HCT emissions, ppm
Visible emissions,
% opacity
1
1-11-72
108
0.550


2880
314,000

59
1.93
12.8
4.8
0.0
<0.3
4.2
<3.8
<10

2
1-12-72
108
0.560


2550
273,000

59
1.92
12.6
4.7
0.0
<0.3
5.7
<2.9
. <10

3
1-12-72
108
0.560


2660
285,000

59
2.23
11.5
6.4
0.0
<0.3
6.4
<4.1
<10

Average

108
0.557


2700
291 ,000

59
2.03
12.3
5.3
0.0
<0.3
5.4
<3.6
<10

Partlculate emissions

     Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
0.024
0.023
0.583
1.06

0.032
0.031
0.779
1.42
0.005
0.005
0.116
0.207

0.007
0.007
0.160
0.286
0.004
0.004
0.099
0.177

0.010
0.010
0.227
0.405
0.011
0.011
0.266
0.481

0.0163
0.016
0.389
0.704
SUMMARY OF RESULTS"
Run number

Date

Test time, minutes

Furnace feed rate,
     ton/hr dry solids

Stack effluent

     Flow rate, dscfm
     Flow rate, dscf/ton
                feed
     Temperature, °F
     Water vapor, vol. t
     COj, vol. % dry
          (less aux. fuel)
     S02 emissions'3

Visible emissions
     Ringelmann No.

Participate emissions

     Total catch

          gr/dscf
1
5-3-71
60
0.325
3480
642,500
80
3.4
4.0
2
5-4-71
60
0.325
3600
664,600
80
3.4
5.1
3
5-4-71
60
0.325
3320
612,900
78
3.4
4.0
Average

60
0.325
3470
640,600
79
3.4
4.4
                                                                                                                                       <1
         0.020
                                                                                                                   (cor.  to m CO,)
                                                                                                                 gr/acf           f   0.019
                                                                                                                 Ib/hr                0.596
                                                                                                                 Ib/ton of feed       1.84
                     0.031

                     0.029
                     0.956
                     2.94
                                                                                                                                                               <1
0.048

0.047
1.365
4.20
0.033

0.032
0.972
2.99
                                                                                                       aTested by local  agency using Code Method 1.   Probe and filter catch
                                                                                                       not analyzed separately.
                                                                                                       bNo S02 detected.
                                                                                                       C0pac1ty was not recorded.
                                  62
                                                                                                                                          63
                                                                                                                                                             •£

-------
Table A-47.  SLUDGE INCINERATOR FACILITY B,

            SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Furnace feed rate,
tons/hr dry solids
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
feed
Temperature, "F
Hater vapor, vol. %
C02, vol. % dry
0?, vol. % dry
CO, vol . * dry
S02:em1ssions, ppm
NOX emissions, ppm
HC1 emissions, ppm
Visible emissions,
X opacity
1
10-13-71
120"
0.237


3300
835,000
198
3.64
3.8
17.3
0.0
2.29 to 2.57
--
<10

2
10-14-71
120
0.236


2950
750,000
196
4.02
4.7
1.40
0.0
2.75
--
<10

3
10-14-71
120
0.249


2120
511,000
199
3.65
2.7
15.8
0.0
44.2 to 24.3
14.3
0.624 to 1.33
0.621
<10

Average

120
0.241


2790
699,000
198
3.77
' 3.7
15.7
0.0
2.53
27.6
0.858
<10

Partlculate emissions

     Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
0.0245
0.0187
0.690
2.91

0.0374
0.0289
1.06
4.47
                                           0.0196
                                           0.0155
                                            0.495
                                            2.10
                                           0.0374
                                           0.0287
                                            0.945
                                            4.00
                                                0.0173
                                                0.0132
                                                 0.315
                                                 1.26
                                                0.0457
                                                0.0348
                                                 0.832
                                                 3.34
0.0205
0.0158
 0.500
 2.09
0.0402
0.0308
 0.946
 3.94
                                   64
                                                                                                                  Table A-48.  SLUDGE INCINERATOR FACILITY C.

                                                                                                                              SUMMARY OF RESULTS
Run number
Date
Test tine, minutes
Furnace feed rate,
tons/hr dry solids
Stack effluent
• Flow rate, dscfm
Flow rate, dscf/ton
feed
Temperature, °F
Water vapor, vol . %
CO, ; vol . % dry
02. vol. % dry
CO, vol. % dry .
502 emissions, ppm
NOX emissions, ppm

HC1 emissions, ppm
Visible emissions,
% opacity
1
7-15-71
80
0.111


1230
665,000

80
3.23
10.0
7.7
0.0
15. 9. to 11.9
402 to 140

3.50 to 2.62
<10

2
7/15/71
80
0.149


1490
600,000

80
3.00
10.1
7.3
0.0
14.5 to 14.6
90.8 to 74.3

2.33 to 2.62
<10

3 .
7-16-71
80
0.146


1400
575,000

77
2.95
10.2
7.4
0.0
14.6 to 13.3
14.5 to 142
50.6 to 61.8
2.52 to 2.62
<10

Average

to
0.135


1373
613,000

79
3.06
1-0.1
7.5
0.0
14:2
163

2.72
<10

                                                                                               Particulate emissions

                                                                                                    Probe and filter catch
gr/dscf
• gr/acf
Ib/hr
Ib/ton of feed
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
0.0127
0.00985
0.127
1.14

0.0195
0.0150
0.206
1.86
0.0620
0.0477
 0.620
 4.16
0.0696
0.0535
 0.889
 5.97
0.0196
0.0152
 0.196
 1.34
0.0260
0.0201
 0.312
 2.14
0.0314
0.0242
 0:314
 2.21
0.0384
0.0295
 0.469
 3.23
                                                                                                                                           65

-------
Table A-49.  SLUDGE INCINERATOR FACILITY  0,



            SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Furnace feed rate,
tons/hr dry solids
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
feed
Temperature, "F
Water vapor, vol. %
CO?, vol. % dry
02, vol. % dry
CO, vol. % dry
S02 emissions, ppm 8
NOX emissions, ppm
HC1 emissions, ppm 0.
Visible emissions,
% opacity
Particulate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
1
7-21-71
120
0.255


1190
280,000

99
3.92
8.8
6.3
0.0
.29 to 11.2
154 to 168
780 to 260
<10



0.0551
0.0468
0.562
2.20

0.0665
0.0565
0.678
2.66
2
7-21-71
96
0.237


1170
296,000

99
4.09
9.9
7.4
0.0
14.8 to 14.8
41.2 to 42.9
4.16 to 1.56
<10



0.0766
0.0650
0.768
3.24

0.0859
0.0729
0.861
3.63
3
7-22-71
96
0.202


1240
368,000

95
3.48
9.1
8.2
0.0
14.2 to 15.4
17.8
187 to 170
161
2.35 to 2.09
<10



0.0545
0.0467
0.579
2.87

0.0653
0.0559
0.694
3.43
Average

104
0.231


1200
315,000

98
3.83
9.3
7.3
0.0
13.8
132
2.26
<10



0.0621
0.0528
0.636
2.77

0.0726
0.0618
0.744
3.24
                          66
Table A-50.  SLUDGE INCINERATOR FACILITY E,



            SUMMARY OF RESULTS
Run number
Date
Test time, minutes
Furnace feed rate,
tons/hr dry solids
Stack effluent
Flow rate, dscfm
Flow rate, dscf/ton
feed
Temperature, °F
Water vapor, vol. %
C02, vol. % dry
02, vol. % dry
CO, vol. % dry
502 emissions, ppm
NO, emissions, ppm 62
HCl emissions, ppm
Visible emissions,
% opacity
Particulate emissions
Probe and filter catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
Total catch
gr/dscf
gr/acf
Ib/hr
Ib/ton of feed
1
8-5-71
96
0.689


9840
—

135
16.3
4.2
14.9
0.0
2.01
.8 to 46.0
11.9
<10



0.0260
0.0196
2.19
3.18

0.0335
0.0252
2.83
4.11
2
8-5-71
96
0.855


8510
--

145
18.6
4.3
14.9
0.0
2.07
83.5 to 75.8
6.83
<10



0.0136
0.0099
0.99
1.16

0.0221
0.0159
1.61
1.88
3
8-5-71
96
0.290


10,290
--

145
14.8
2,2
16.9
0.0
2.12
44.3 to 54.7
10.9
<10



0.0134
0.0101
1.18
4.07

0.0170
0.0128
1.50
5.17
Averagt

96
0.611


9547
—

142
16.6
3.6
15.6
0.0
2.07
61.2
9.88
<10



0.0177
0.0132
1.45
2.80

0.0242
0.180
1.98
3.72
                                                                                                                                 67

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