4>EPA
            United States
            Environmental Protection
            Agency
            Environmental Research
            Laboratory
            Corvallis OR 97330
EPA-600/3-81-007
February 1981
            Research and Development
The
Bioenvironmental
Impact of a Coal-
Fired Power Plant

Sixth Interim Report,
Colstrip, Montana
August 1980

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                                 DISCLAIMER

     This report has been reviewed by the Corvallis Environmental Research
Laboratory,  U.S. Environmental Protection Agency,  and approved for publica-
tion.  Mention of trade names or commercial products does not constitute
endorsement or recommendation for use.
                                     ii

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                                    PREFACE
     The Environmental  Protection Agency  has  funded research for use  in as-
sessing potential  impacts of  coal-fired  power plant  siting in the  northern
Great Plains.   Planners need  to  be able to predict environmental  impacts  of
power plants  when  evaluating  construction  proposals.   Power plant  managers
need environmental monitoring  methods  to  warn of developing ecological  damage
in  time  for mitigation  efforts to be  effective.   The project  rationale and
design was  presented in  detail in introductory sections of previous  interim
reports.

     The project activities  include monitoring of ecological effects  from two
350 megawatt coal-fired power plants at Colstrip,  Montana  as well as  field and
laboratory process studies designed to elucidate the mechanisms  responsible  for
ecological effects from power plant emissions.

     Pre-construction  documentation of  the  environmental  characteristics  of
the  grassland  ecosystem  in the  vicinity  of  Colstrip, Montana  began  in the
summer of 1974.  This documentation continued until Colstrip generating  unit 1
began operation  in  September,  1975.   Since  then  key  characteristics  of the
ecosystem have been  monitored  regularly to detect possible  pollution  impacts.

     In 1974,  a  Zonal Air Pollution System  (ZAPS)  was  designed  to  stress 0.5
hectare areas of native grassland with measured concentrations of S02 •   In the
summer of  1975,  field  stressing  experiments  were  begun  to  provide  the  data
necessary  to  develop  dose-response models  of S02 stresses on a  grassland
ecosystem.  A  second Zonal Air Pollution System (ZAPS  II),  was  constructed  in
1976.  Both ZAPS I  and ZAPS  II  were operated during the  growing  seasons  of
1976, 1977, 1978, and 1979.  The  design of these experimental systems has been
described in previous interim  reports.  Their  behavior is further described in
the present report.

     Methodologies used in evaluating the effects of S02 on grassland plants
and animals is presented in Sections 1 through 3 of the report.   Sections 4
through 12  report  results  of research concerning the  effects of S02  exposure
on  energy  flow  and nutrient  cycling  in  grasslands,  Sections  13 through  17
describe  the  effects  of  chronic  S02  exposure  on  population   and  community
structure, and Sections 18 through 23 describe research concerning potentially
useful  bioindicators and  biomonitors  of  coal-fired  power  plant  emissions.
                                      iii

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                                   ABSTRACT

     The grasslands of the northern plains consist of a complex combination of
interacting plant  and  animal  species that capture, store,  and utilize energy
in a  self-sustaining manner.   Pollution  stress on these rangelands may affect
a variety of ecological processes.

     The  Coal-Fired  Power Plant  Project at Colstrip  is  designed  to evaluate
the environmental  impact  of  air emissions from coal-fired power plants in the
northern Great Plains ecosystems.  The project consists  of three parts:

      (1)  A case study of the ecological impact of two 350 megawatt coal-fired
          generating units at  Colstrip, Montana.

      (2)  A series of  field  and laboratory process studies designed to elabo-
          rate the mechanism of 863 action on grasslands chronically fumigated
          at low levels.

      (3)  Development  of  a methodology  for incorporating  ecological  effects
          information into the power plant siting process.

     Documentation  of  the  environmental  characteristics  of the  grassland
ecosystem  in  the  vicinity of Colstrip,  Montana began in the  summer of 1974.
This  continued  until  Colstrip generating Unit 1 began operation  in September,
.1975.  Since then, key characteristics of the ecosystem have been monitored to
detect  air pollution and its  ecological  effects.  This  report summarizes the
results of the 1979 field season.
Methodology

     In 1974,  a  Zonal Air-Pollution System  (ZAPS)  was  designed to stress 0.5
hectare areas  of native grassland with measured concentrations of S02.  Field
stressing experiments were initiated during the summer of 1975.  A second ZAPS
was  constructed  in 1976.   Both ZAPS I and ZAPS II were operating during 1976,
1977, 1978,  and 1979.

     During the  1979  field season, the geometric mean 802 concentrations were
0.8-1.4, 2.4-2.6,  4.9,  and 7.3 pphm on'ZAPS  I and 0.9-1.4, 2.4-2.6, 5.0-5.1,
and  9.5-9.7 pphm on ZAPS II for the Control, Low, Medium, and High treatments,
respectively.  These  concentrations were  similar  to those  of past  years  of
fumigation.

     For  laboratory experiments an exposure chamber  is  described for studies
of  long-term  (2-4 months)  S02 effects on  organisms (i.e.  grasshoppers and
microorganisms)  involved  in plant  litter  decomposition.  Also  described is a
relatively  inexpensive  physiological  activity and diagnostic chamber designed
to measure foliar exchange rates of 862, 1^0,  and C02 in grass leaves.

                                     iv

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Energy Flow and Nutrient Cycling

     Several  field  and  laboratory  studies  were conducted  to  evaluate  the
effects  of S02  exposure  on energy  flow and  nutrient  cycling in  the native
grassland  ecosystem.   The experiments  were  specifically designed  to provide
information  required  to  improve  simulation models  of  S02  effects  on system
processes that are under development.

     In  an  exposure  chamber  experiment,  translocation of  photoassimilated
14C02  by  individual  source  leaves  of  Agropyron sm-ifhii.  were stimulated  by
exposure  of  the  plants  to  10 pphm S02.   Leaves near  the  top  of  the plant
supplied  proportionately  more  assimilate  to  the  developing  leaf  than  to
rhizomes.   Lower  leaves partitioned  a greater proportion to  a S02 stimulated
rhizome  sink.  Sulfur  dioxide exposure  increased  14C  concentrations  in  the
belowground  compartment only  on  the first sampling date.   The initiation of
tillers  is  probably similar to that of  developing  leaves  and requires carbon
import until self-sustaining photosynthetic  capacity is reached.

     A laboratory  chamber experiment exposing western wheatgrass  litter to 8.5
pphm for 5 weeks showed a 9-17 percent reduction  in decomposition rates under
S02 exposure  compared to  controls.  Lowered pH conditions in the litter may
have been responsible for reduced microbial activity.

     It was hypothesized  that  S02 exposure of the ZAPS sites was  stressing the
western  wheatgrass population and  that by  subjecting  the population  to  an
additional  stress  (simulated grazing),  a large negative effect on the popula-
tion would  be observed.  Results of a field experiment  failed to support this
hypothesis.   The  only  responses  observed could  have  resulted from the simu-
lated grazing alone and did not suggest synergism with S02 exposure level.

     Bouteloua gz>aoi1is,  an important warm  season grass native  to the Great
Plains  of North  America,  was grown hydroponically  on  Low,  Medium,  and High
treatments  on the  ZAPS.   After  31 days  exposure, plants  showed  no treatment
effect  on  live  shoot  weights, net  weights,  shoot:root ratios,  or number of
tillers.   However,  crown weight  significantly decreased and  live:dead  shoot
ratios increased on the lowest treatment plot and decreased on Medium and High
treatments.

     Leaching by  precipitation  influences estimates  of  sulfur  accumulation
rates.  Such  leaching  from western wheatgrass tillers on the  ZAPS High treat-
ment was estimated to be 5-13 percent depending upon the time of exposure.
Over-winter loss of plant sulfur was estimated to be 54 and 74 percent for
Control and S02 exposed tillers,  respectively.  Accounting for rainfall leach-
ing increased ability to predict live plant sulfur concentration by 6 percent.

     Chlorophylls  a and  b in  eight species of grassland plants exposed to S02
on  ZAPS  were  increased,  unchanged,  or  decreased depending upon S02 concen-
tration  and  species.   Chlorophyll a  was most  sensitive to  exposure but the
degree of sensitivity was  species specific.

     Sulfur distribution  in western wheatgrass exposed to S02  on  the  ZAPS High
treatment under various root sulfur availability  regimes was studied  to deter-

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 mine the  interactive  effects of  atmospheric  and substrate  sulfur on  sulfur
 metabolism.   Sulfur dioxide  exposure  had no  effect  on shoot and  root  sulfur
 content.   Root sulfur  availability significantly affected  plant  sulfur  con-
 tent.   Shoot/root  ratios  were  greater  early in the  season  on  S02  exposed
 plants  but the trend  late  in the season suggested reduced  root  growth rather
 than increased  shoot  growth.   Nitrogen fertilization of western  wheatgrass
 exposed to S02  on the ZAPS  treatments  appeared  to  ameliorate the  effects  of
 S02  exposure  and  increased  the  rate  of senescence  with increasing levels  of
 S02  exposure.

      Soil  samples  from the ZAPS  High  treatment had 6  times the sulfur con-
 tent of those from the Control plot.


 Population and Community Structure

      Germination   and   establishment   in the   greenhouse  were  significantly
 reduced on soils  from the High  treatment for  five  grassland  species.   Non-
 graminoids were particularly reduced.   Volunteer weeds were more abundant and
 diverse on soils from  the  Control and Low treatment plots  than  on the Medium
 and  High treatment plots.

      Neither  nematodes nor rotifers were measurably  affected by  S02  exposure
 on  the  ZAPS  plots,   though  soil microarthropod  groups  were  significantly
 reduced.   These reductions were  not  large enough  to affect the  total  micro-
 arthropod  population  distribution.  Most population  reduction  occurred in the
 first  half of the growing  season when soil water  conditions were  highest.
 Significant population reductions were  also observed in some  groups of above-
 ground  arthropods, but these were not  large enough  to  cause a  significant
 change  in overall aboveground  arthropod population.

     An exposure  chamber  study of  the effects of 17  pphm S02  on  the migratory
 grasshopper Melanoplus sanguinipes  (Fab.)   showed  no  significant  difference
 between Control and S02 exposed individuals in egg viability,  mean developmen-
 tal  time for each nymphal instar,  adult dry weight biomass,  and egg production
 per  female per day.  This  suggests that previously reported population reduc-
 tions of this  species on certain  ZAPS treatments were  not  due  to  direct toxic
 effects.   The  reported population reductions  may have  resulted from migration
 off the treatment sites.
Bioindicators and Biomonitors

     Lichens  are  used  throughout  the world  as  bioindicators of air quality.
Since 1975, various  characteristics of native  lichens  have been monitored at
various  distances  from  Colstrip.   In  1979,  respiration  rates,  chlorophyll
content, and rate  of photosynthesis  in two lichen species ( Usnea hirta and Par-
melia ohloroohroa ) had no  significant linear relationship with distance from
Colstrip.  However, sulfur content  of Usnea hirta significantly decreased with
increased distance  from Colstrip.  If Colstrip  emissions have had any  impact
on lichens in  the vicinity, it has been slight.


                                     vi

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     Anatomical  and physiological  responses  of  Usnea hirta and Parmelia ohlo-
TOchvoa transplants on the ZAPS plots were measured to determine SC>2 dose/re-
sponse relationships for these two species.  Significant reductions in respir-
ation rate in Usnea hirta occurred on the Low plot after 100 days exposure.
Reductions in pigment content and increases in plasmolyzed algal cells occurred
within 90 days.  On the Medium treatment, respiration rates decreased and algal.
cell plasmolysis increased within 60 days.  Parmelia chloTOohToa exposed near
the soil surface showed no detectable response,

     Managed  honey bees  appear  promising for  use  as biological  monitors of
coal-fired  power  plant  emissions.  Since  1974,  honey  bees  from commercial
apiaries  in  the Colstrip area have been sampled  and analyzed for fluoride, a
toxicant released by coal combustion.

     Honey  bees  in  the vicinity  of  Colstrip,  Montana  showed  significant
increases  from  fluoride levels  in 1977  and  1978.   Patterns of  fluoride in
pollen  and  the geographical distribution of fluoride  buildup  with respect to
Colstrip and prevailing  winds suggest airborne rather than waterborne fluoride
exposure.

     Baseline  histological  information  on  western  meadowlark and  the deer
mouse was  gathered for  later comparison  with  data  gathered after power plant
operation.  These  histological studies describe seasonal cycles in body compo-
sition, organ system function, and energetics.

     Western  meadowlark lungs collected  in  the vicinity  of Colstrip, Montana
were  examined  for particulates during  1975 (before plant  operation), 1976,
1977, and  1978.  Three types of particles were observed including crystals of
variable  size,  very  small  (<_  0.47  urn) round black  flecks and  large black
particles  of  round or  irregular shape.  Particulate burdens increased steadily
between  1975  and 1977 and were similar  for  male  and female birds.  Juveniles
had a smaller burden than adults.
                                     vii

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                                   CONTENTS

Preface	

Abstract	     iv

List of Contributors	    X11

Acknowledgements  	    xi-v


SECTIONS

                                  METHODOLOGY

1.   Temporal Variation in S02 Concentrations on ZAPS During 1979
          T.J. McNary	      1

2.   Design and Construction of a Simple, Continuous Flow Sulfur
     Dioxide Exposure Chamber
          J.W. Leetham, W. Ferguson, J.L. Dodd, and W.K. Lauenroth  .   .     10

3.   A System for Measuring Foliar Exchange Rates Under
     Environmentally Controlled Conditions
          S.R. Bennett, J.L. Dodd, W.S. Ferguson, C.J. Bicak,
          G.L. Thor, and W.K. Lauenroth	     16


                        EFFECTS OF CHRONIC S02 EXPOSURE
                          ON ENERGY FLOW AND NUTRIENT
                             CYCLING IN GRASSLANDS

4.   The Effects of S02 on 14C Translocation in Western Wheatgrass
          D.G. Milchunas, W.K. Lauenroth, and J.L. Dodd	     27

5.   Effects of LowKLevel Sulfur Dioxide Exposure on Decomposition
     of Western Wheatgrass (Agropyrcm smtt/zii) Litter under
     Laboratory Conditions
          J.W. Leetham, J.L. Dodd, and W.K. Lauenroth	     43

6.   Impact of S02 Exposure on the Response of Western Wheatgrass
     (Agropyron smi-thii) to Defoliation
          W.K. Lauenroth, J.K. Detling, and J.L. Dodd	     49
                                       ix

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 7.  Response of Bouteloua gracilis  to Controlled S02 Exposure
          W.K. Lauenroth,  J.K.  Detling, C.J.  Bicak, and J.L.  Dodd ...     59

 8.  The Impact of Sulfur  Dioxide on the Chlorophyll Content
     of Grassland Plants
          W.K. Lauenroth and J.L. Dodd	     66

 9.  Adherence of Water to Leaf Surfaces of Agropyron smith-Li
          J.L. Dodd and J.E. Heasley	     74

10.  The Influence of Precipitation on the Sulfur Concentration
     of Agpopyron smithii  Rydb. Exposed to Sulfur Dioxide
          D.G. Milchunas,  J.L.  Dodd, J.E.  Heasley, and W.K.  Lauenroth .     76

11.  Sulfur Distribution and Allocation in Western Wheatgrass
     Exposed to S02 Under  Variable Nutrient Sulfur Regimes
          C.J. Bicak, W.K. Lauenroth, and J.L.  Dodd	     83

12.  Effects of S02 Exposure with Nitrogen and Sulfur Fertilization
     on the Growth of Agropyvon smithii Rydb.
          D.G. Milchunas,  W.K.  Lauenroth,  J.L.  Dodd, and T.J. McNary  .     96


                            EFFECTS OF CHRONIC S02
                            EXPOSURE ON POPULATION
                            AND COMMUNITY STRUCTURE

13.  Germination and Seedling Establishment as Affected by
     Sulfur Dioxide
          W.C. Leininger and J.E. Taylor	    115

14.  Response of Field Populations of Soil Nematodes and Rotifers
     to Three Levels of Season-Long Sulfur Dioxide Exposure
          J.W. Leetham, T.J. McNary, J.L.  Dodd, and W.K. Lauenroth  .  .    131

15.  Arthropod Population  Responses to Three Levels of Chronic
     Sulfur Dioxide Exposure in a Northern Mixed-Grass Ecosystem.
     I. Soil Microarthropods
          J.W. Leetham, J.L. Dodd, R.D. Deblinger, and W.K.  Lauenroth .    139

16.  Arthropod Population  Responses to Three Levels of Chronic
     Sulfur Dioxide Exposure in a Northern Mixed-Grass Ecosystem.
     II. Aboveground Arthropods
          J.W. Leetham, J.L. Dodd, R.D. Deblinger, and W.K.  Lauenroth .    158

17.  Response of Melanoplus sanguinipes to Low-Level Sulfur
     Dioxide Exposure from Egg Hatch to Adult (Orthoptera:
     Acrididae)
          J.W. Leetham, J.L. Dodd, J.A. Logan, and W.K. Lauenroth ...   176
                                       x

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                              POTENTIALLY USEFUL
                         BIOINDICATORS AND BIOMONITORS
                              OF COAL-FIRED POWER
                                PLANT EMISSIONS

18.  Observations on Two Lichen Species in the Colstrip Area,  1979
          S. Eversman	     185

19.  Effects of Low-Level S02 on Two Native Lichen Species;
     1979 ZAPS Observations and Project Summary
          S. Eversman	     198

20.  Fluoride and Arsenic Concentrations in Honey Bees Near
     Colstrip
          J.J. Bromenshenk	     210

21.  Baseline Histology of Selected Organs of the Deer Mouse,  Peromyscus
     maniaulatus, in Rosebud County, Montana
          M.D. Kern and R.A. Lewis	     228

22.  Seasonal Cycles in Body Composition, Organ System Function and
     Energetics of the Western Meadowlark in Southeastern Montana:
     A Report of Progress
          M.L. Morton, R.A. Lewis, and E. Zerba	     274

23.  Particulates in the Lungs of Western Meadowlarks
     (Sturnella neglecta) in Southeastern Montana
          M.D. Kern, R.A. Lewis, and M.B. Berlin	     315
                                      XI

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                              LIST  OF  CONTRIBUTORS
 S.R.  Bennett
 Natural Resources  Ecology Laboratory
 Colorado State University
 Fort  Collins,  Colorado 80521

 M.B.  Berlin
 Department of  Biology
 The College of Wooster
 Wooster, Ohio  44691

 C.J.  Bicak
 Natural Resources  Ecology Laboratory
 Colorado State University
 Fort  Collins,  Colorado 80521

 J.J.  Bromenshenk
 Natural Resources  Ecology Laboratory
 University of  Montana
 Missoula,  Montana  59801

 R.D.  Deblinger
 Natural Resources  Ecology Laboratory
 Colorado State University
 Fort  Collins,  Colorado 80521

 J.K.  Detling
 Natural Resources  Ecology Laboratory
 Colorado State University
 Fort  Collins,  Colorado 80521

 J.L.  Dodd
 Natural Resources  Ecology Laboratory
 Colorado State University
 Fort  Collins,  Colorado 80521

 S. Eversman
 Department of  Biology
 Montana State  University
 Bozeman, Montana 59715

 W.S.  Ferguson
 Natural Resources  Ecology Laboratory
 Colorado State University
Fort  Collins,  Colorado 80521
J.E. Heasley
Natural Resources Ecology Laboratory
Colorado State University
Fort Collins, Colorado 80521

M.D. Kern
Department of Biology
The College of Wooster
Wooster, Ohio 44691

W.K. Lauenroth
Natural Resources Ecology Laboratory
Colorado State University
Fort Collins, Colorado 80521

J.W. Leetham
Natural Resources Ecology Laboratory
Colorado State University
Fort Collins, Colorado 80521

W.C. Leininger
Department of Animal and Range Sciences
Montana State University
Bozeman, Montana 59715

R.A. Lewis
Ecological Research Division
Office of Health and
  Environmental Resources
Department of Energy
Washington, D.C. 20545

J.A. Logan
Natural Resources Ecology Laboratory
Colorado State University
Fort Collins, Colorado 80521

T.J. McNary
Natural Resources Ecology Laboratory
Colorado State University
Fort Collins, Colorado 80521
                                     xii

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D.G. Milchunas
Natural Resources Ecology Laboratory
Colorado State University
Fort Collins, Colorado 80521

M.L. Morton
Department of Biology
Occidental State College
1600 Campus Road
Los Angeles, California 90041

D.W. O'Guinn
U.S. EPA/CERL
200 S.W. 35th Street
Corvallis, Oregon 97330

E.M. Preston
U.S. EPA/CERL
200 S.W. 35th Street
Corvallis, Oregon 97330
J.E. Taylor
Department of Animal and Range Sciences
Montana State University
Bozeman, Montana 59715

G.L. Thor
Natural Resources Ecology Laboratory
Colorado State University
Fort Collins, Colorado 80521

R.A. Wilson
U.S. EPA/CERL
200 S.W. 35th Street
Corvallis, Oregon 97330

E. Zerba
Department of Biology
Occidental State College
1600 Campus Road
Los Angeles,  California 90041
                                    xiii

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                               ACKNOWLEDGEMENTS

     Many  individuals  have contributed  to  the preparation  of  this document.
The editorial  assistance of  Karen Randolph and  others is  much  appreciated.

     Our work  could  not proceed without the help and support of the people of
southeastern Montana, especially the ranchers on whose land we are working and
the personnel  and  persons residing  at and near  Fort Howes Ranger  Station,
Custer National Forest.   The  Kluver's and the McRae's  have  been  particularly
supportive.
                                     xiv

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                                 METHODOLOGY
                                  SECTION 1

       TEMPORAL VARIATION IN S02 CONCENTRATIONS ON ZAPS DURING 1979

                                 T. J. McNary


                                  ABSTRACT

               The Zonal Air Pollution System (ZAPS) was designed
          to deliver atmospheric S02 pollution on a small portion
          of the prairie ecosystem in Montana.  Geometric mean
          S02 concentrations were 0.82-1.41, 2.44-2.59, 4.88-4.92,
          and 7.32-7.35 pphm for the Control and Low-, Medium-,
          and High-S02 plots, respectively,  on ZAPS I and
          0.87-1.39, 2.42-2.64, 5.01-5.15, and 9.52-9.73 pphm on
          ZAPS II.  Except for the high-S02  plot, S02 concentra-
          tions were similar to those of past years of fumigation.
          Diel patterns showed much greater  S02 concentrations
          at night than during the day, and  indicated that diel
          activity patterns of organisms must be considered when
          evaluating dose-response relationships.
                               INTRODUCTION

     The ZAPS consisted of two 11-ha exclosures in the mixed-grass prairie
of southeastern Montana, in the Ashland Division of Custer National Forest.
The system was designed for experimental evaluation of the effects of long-
term, low-level exposure to sulfur dioxide.  Parameters evaluated included
plant and animal community structures, insect population and behavior,
pollination systems, lichens, physiological functions, and biochemical
functions.

     Each exclosure contained four 0.5-ha plots, each receiving a different
fumigation level of S02.  The four plots were designated control (A), Low
(B), Medium (C), and High (D) to describe the relative level of S02 received.
The S02 was distributed over each plot through a network of aluminum pipes
suspended about 75 cm above the soil surface.  Gas-release orifices (0.8 mm
dia.) were positioned at 3-m intervals, with more than 250 orifices on each
plot.  No locus on a plot was more than 5.5 m from an orifice.  A detailed
description of the design of the ZAPS is presented by Lee et al, (1976), Lee
and Lewis (1978), Lee et al. (1979), and Preston et al. (1980).

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     Although  controls  did  not receive  S02  through  the network of pipes,  the
controls were  exposed to  SC>2  that  drifted from upwind plots.  Consequently,
controls received  low-level,  periodic S02 fumigation that resembled  exposure
from a point source rather  than from an area source.  Sulfur dioxide was
applied to treatment plots  throughout the growing season (April-October); fum-
igation began on ZAPS I in May 1975 and on ZAPS II in April 1976.  Sulfur di-
oxide exposure was at a constant rate but concentrations within plots varied
with meterological conditions, primarily wind speed.

     In this section temporal variation in  S02 concentration is  characterized.

                              MATERIALS  AND  METHODS

     Sulfur dioxide concentration  was measured at a central locus on each
plot with  a Meloy  Laboratory  Sulfur Analyzer  (Model SA 160-2) on a time-
sharing basis  throughout  the  season.  Ambient air samples were measured at 35
cm  above the ground, which  is close to  canopy height for this type of grass-
land.

     In general, the procedures described in Lee et ol,  (1979) modified by
Preston &t at,  (1980) were  followed in  1979.  Span  checks of the analyzer were
performed  semi-weekly,  and  calibrations adjusted when needed.

     Calibration curves that  related analyzer response to logarithms of S02
concentration  became nonlinear at  concentrations below 2 pphm.   Therefore,
linear extrapolation led  to an overestimation of S02 levels in the 0-2 pphm
range.  True values were  probably  between 0.1 pphm  and the value estimated
from the calibration curve.  During data analysis,  each analyzer response was
entered into  two calibration  equations.  The High run was adjusted to yield a
maximum value  that could  result from the above-mentioned sources of  uncertain-
ty. The Low run yields the corresponding minimum value for the  S02  concentra-
tion.  Summary statistics were computed for both the High and Low runs.

                            RESULTS AND DISCUSSION

Interseasonal  Trends

     A seasonal summary of  S02 concentration for ZAPS I and ZAPS II  for 1979
is  presented  in Tables  1.1 and 1,2.   The  first number for each entry is for
the Low run value  and  the second number is  for the High run value.   If only
one number appears,  there was no difference between the Low and High run
values.

      Sulfur dioxide  concentrations for  the  Control, Low, and Medium  plots in
 1979 were  similar  to  those  in past years  (Table 1.3).  For Low-S02 plots, con-
centrations declined  slightly from the  peaks in 1977.  Trends of increasing
 S02 on High  plots over the years  continued for ZAPS II and reached  a geo-
metric mean of 9.52-9.73  pphm in 1979.  This trend  was dramatically  reversed
on  the ZAPS I  High-S02  plot,  where the  S02  concentration decreased to a geo-
metric mean of 7.32-7.35  pphm. For more information on S02 concentrations in
past years, see Preston et  al. (1980) for 1978 data and Lee et at.  (1979) for
 1977  and  1976  data.

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TABLE  1.1.  ZAPS I SEASONAL SUMMARY, 1979*
Treatment
         Geometric
           mean
Standard
geometric
deviation
                                                            Arithmetic
                                                               mean
Control
         0.82-1.41
3.49,1.63
Low
Medium
High
            1-hour ave. exceeded 25 pphm
            3-hour ave. exceeded 50 pphm
           24-hour ave. exceeded 10 pphm
           24-hour ave. exceeded 14 pphm
                                     0 times:
                                     0 times;
                                     0 times;
                                     0 times;
1.47-1.69

   0 percent
   0 percent
   0 percent
   0 percent
        1-hour peak:  19.12    3-hour peak:  13.24    24-hour peak:   5.25
         2.44-2.59           2.43,3.49

 1-hour ave. exceeded 25 pphm     19.0 times:
 3-hour ave. exceeded 50 pphm        0 times:
24-hour ave. exceeded 10 pphm      2.0 times;
24-hour ave. exceeded 14 pphm        0 times;
                    3.70-3.73

                     .48 percent
                       0 percent
                    1.10 percent
                       0 percent
        1-hour peak:  47.41    3-hour peak:  27.79    24-hour peak:  13.47
         4.88-4.92           2.55,2.49

 1-hour ave. exceeded 25 pphm     203.0 times:
 3-hour ave. exceeded 50 pphm       1.0 times;
24-hour ave. exceeded 10 pphm      40.0 times;
24-hour ave. exceeded 14 pphm      13.0 times;
                    8.52

                     5.09 percent
                      .07 percent
                    21.98 percent
                     7.14 percent
        1-hour peak:  87.49    3-hour peak:  52.65    24-hour peak:  28.41
         7.32-7.35
2.41,2.37
             1-hour ave. exceeded 25 pphm    471.0 times:
             3-hour ave. exceeded 50 pphm     18.0 times:
            24-hour ave. exceeded 10 pphm     91.0 times;
            24-hour ave. exceeded 14 pphm     49.0 times;
11.62

11.82 percent
 1.33 percent
50.00 percent
26.92 percent
        1-hour peak:  138.12   3-hour peak:  88.80    24-hour peak:  37.92
*  pphm S02 monitored near treatment center at canopy height.

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 TABLE   1.2.   ZAPS  II  SEASONAL  SUMMARY,  1979*
 Treatment
         Geometric
           mean
Standard
geometric
deviation
Arithmetic
   mean
 Control
         0.87-1.39
2.89,1.27
Low
Medium
High
             1-hour  ave.
             3-hour  ave.
            24-hour  ave.
             exceeded 25 pphm
             exceeded 50 pphm
             exceeded 10 pphm
            24-hour  ave.  exceeded  14 pphm
     0 times:
     0 times:
     0 times:
     0 times:
1.24-1.45

0 percent
0 percent
0 percent
0 percent
         1-hour  peak:   19.43     3-hour peak:  10.34    24-hour peak:  2.34
         2.42-2.64
2.56,2.07
              1-hour ave. exceeded 25 pphm    5.0 times;
              3-hour ave. exceeded 50 pphm    0   times:
            24-hour ave. exceeded 10 pphm    2.0 times:
            24-hour ave. exceeded 14 pphm    1.0 times:
3.78-3.82

0.18 percent
0    percent
1.18 percent
0.59 percent
         1-hour peak:  39.78    3-hour peak:  25.71    24-hour peak:  18.13
         5.01-5.15           2.71,2.50

 1-hour ave. exceeded 25 pphm
 3-hour ave. exceeded 50 pphm
24-hour ave. exceeded 10 pphm
24-hour ave. exceeded 14 pphm
                                             168.0 times:
                                               0
           times:
                                              40.0 times:
                                              14.0 times:
8.57-8.58

 6.19 percent
 0    percent
23.53 percent
 8.24 percent
        1-hour peak:  60.65    3-hour peak:  47.36    24-hour peak:  33.40
         9.52-9.73
2.97,2.77
            1-hour ave.
            3-hour ave.
           24-hour ave.
             exceeded 25 pphm
             exceeded 50 pphm
             exceeded 10 pphm
           24-hour ave. exceeded 14 pphm
     487.0 times:
      61.0 times:
     119.0 times:
      83.0 times:
18.13-18.14

17.93 percent
 5.19 percent
70.00 percent
48.82 percent
        1-hour peak:  152.72   3-hour peak:  113.58   24-hour peak:   56.00
   pphm S02 monitored near treatment center at canopy height,

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TABLE   1.3.  ANNUAL  GEOMETRIC MEAN  S02 CONCENTRATION  (PPHM) FOR ZAPS I
             AND  ZAPS  II,  1975-79

Treatment
Year
1975
1976

1977

1978

1979

Site
ZAPS
ZAPS
ZAPS
ZAPS
ZAPS
ZAPS
ZAPS
ZAPS
ZAPS
I
I
II
I
II
I
II
I
II
Control
1
0
0
0
0
1
0
0
0
.0
.2-0
.2-1
.2-1
.4-1
.0-1
.9-1
.8-1
.9-1

.9
.4
.6
.6
.1
.2
.4
.4
1
1
2
3
2
2
2
2
2
Low
.7
.8-2.2
.6-2.9
.2-3.4
.9-3.0
.8
.5
.4-2.6
.4-2.6
Medium
3
3
4
5
4
5
4
4
5
.8
.7-3.9
.1-4.4
.3-5.6
.7-4.9
.1
.6
.9
.0-5.2
High
6
6
6
7
7
8
9
7
9
.7
.5-6.7
.4-6.9
.0-7.5
.5-8.2
.6-8.9
.2-9.3
.3-7.4
.5-9.7

      The frequency of high concentrations  was  less  in  1979  than  in  1978,
except for the High plot on ZAPS II,  which  was  similar  to  that  of  1978  (Fig-
ure 1.1) (Preston et al.,  1980;  Lee et al., 1979).   The data were  presented in
this format for comparison with  previous reports.

 Intraseasonal Trends

      Intraseasonal trends  on ZAPS  I  and ZAPS II were different.  On ZAPS I
 there was  a  slight increase in  S02 concentration on all plots throughout the
 growing season (Figure 1.2).   On  ZAPS II  Control, Low, and hedium plots, S02
 concentration remained relatively  constant.  Concentration on the High plot
 decreased  from April  to June, then increased for the remainder of the season
 (Figure 1.3).

 Diel  Patterns

      Diel  patterns of  S02  concentration on each ZAPS site were similar in
 1979  to previous  years.  Concentrations of S02 were lowest during the day-
 light hours  (Figure  1.4 and  1.5),  probably because of higher wind speeds
 and greater  mixing of  the  air than at night.

-------
              a.
              CL
 Figure   1.1.
                IOO
                  10
                                  ZAPS I
                                   1979
                                             ZAPS  H
                                               1979
    O.I  i   IO  5O   95           O.I I   10   50   95

  CUMULATIVE FREQUENCY ABOVE GIVEN CONCENTRATION (%)

 Frequency distribution of S02  concentration on ZAPS,  1979,
                    2Oi
Figure  1.2.
                                                        Medium
                        I I  I I  II I  I I  II  I I I  I I  I I I
                          4     8     12    16   20
                                  HOUR OF DAY
                                    rn
                                      24
Monthly variation in geometric  mean  S02 concentration on ZAPS
I, 1979 (High  run).

-------
                   20-1
Figure  1.3.
                                                        High
                                                        Medium
        I  || I  I I  I II II I I T I  I I I  I I  I I  I
          4      8     12     16    2O    24

                  HOUR OF DAY



Monthly variation in geometric SC>2 concentration on ZAPS II,

1979 (High run).
Figure   1.4.
               o
                ui
                o

                o  10-
                u

                CM

                8j
               UJ
               o
               cc
               UJ
                                                          High
                                                          Medium
                                                          Low
                                                          Control
                          r
                 i
r
T
    APR  MAY   JUN    JUL   AUG   SEP   OCT


Diel  cycles of SC>2  concentration on  ZAPS  I,  1979 (seasonal

geometric  mean, High run).

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                  151
Figure  1.5.
                                      ZAPS I
                                       1979
                   APR  MAY
                     JUL   AUG   SEP   OCT
Diel cycles of SOa concentration on ZAPS  II,  1979  (seasonal
geometric mean, High  run).
                                  CONCLUSIONS
     Geometric mean S02 concentrations on ZAPS I were 0.82-1.41 (Control),
2.44-2.59 (Low), 4.88-4.92 (Medium),  and 7.32-7.35 (High)  pphm.  Concentra-
tions on ZAPS II were 0.87-1.39 (Control), 2.42-2.64 (Low),  5.0-5.15 (Medium),
and 9.52-9.73 (High) pphm.  Seasonal  S0£ concentrations were similar to pre-
vious years, except for the High plot, where concentrations  increased on ZAPS
II and decreased on ZAPS I.  Sulfur dioxide concentrations were relatively
constant or increased slightly throughout the season, except for the High plot
on ZAPS II.   Sulfur dioxide concentrations were greater at night than during
the day.
                                REFERENCES

Lee, J. J.,  R. A. Lewis, and D. E. Body.  1976.  The Field Experimental
     Component:   Evaluation of the Zonal Air Pollution System.  In:  The
     Bioenvironmental Impact of a Coal-fired Power Plant,  Second Interim
     Report, Colstrip, Montana. N. R. Glass and A. S. Lefohn, eds.   EPA
     600/3-76-013, U.S. Environmental Protection Agency, Corvallis, Oregon.
     pp. 188-202.

Lee, J. J.,  and R. A. Lewis.  1978.  Zonal Air Pollution System.  In:  The
     Bioenvironmental Impact of a Coal-fired Power Plant,  Third Interim
     Report, Colstrip, Montana. E. M. Preston and R. A. Lewis, eds.  EPA-
     600/3-78-021, U.S. Environmental Protection Agency, Corvallis, Oregon.
     pp. 322-344.

-------
Lee, J. J., E. M. Preston, and D. B. Weber.  1979.  Temporal Variation in S02
     Concentration  on ZAPS.  In:  The Bioenvironmental Impact of a Coal-fired
     Power Plant, Fourth Interim Report, Colstrip, Montana. E. M. Preston and
     T. L. Gullett, eds.  EPA 600/3-79-044, U.S. Environmental Protection
     Agency, Corvallis, Oregon,  pp. 284-305.

Preston, E.  M.,  T. L.  Gullett,  and D.  B. Weber.   1980.  Temporal Variation
     in S02 Concentrations on ZAPS During the 1978 Field  Season.   In:  The
     Bioenvironmental Impact of a Coal-fired Power Plant,  Fifth Interim Report,
     Colstrip,  Montana.   E.  M,  Preston and D.  W.  O'Guinn,  eds.   EPA-600/3-80-
     052.  U.S.  Environmental Protection Agency,  Corvallis,  Oregon.   pp.  96-107.

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                                 SECTION 2

                 DESIGN AND CONSTRUCTION OF A SIMPLE,  CONTINUOUS
                      FLOW SULFUR DIOXIDE EXPOSURE CHAMBER

            J.W. Leetham, W.  Ferguson,  J.L.  Dodd,  and  W.K.  Lauenroth
                                    ABSTRACT

               The design and construction of a low-cost,  low-
          maintenance S02 exposure chamber is described.   The
          chamber is designed to be used for organisms other than
          plants and for long exposure periods.  Efficiency of
          the chamber is discussed.
                               _INTRODUCTION

     Most studies of the effects of air pollutants on organisms and/or bio-
logical processes require exposure to controlled levels of the pollutants for
specific time periods.  Since most controlled-exposure studies deal with plants,
the requirements of a system to administer the pollutant exposure are quite
stringent in regards to environmental conditions which affect growth of the
test plants.  These requirements often lead to the construction of expensive
exposure chambers (Heck et at., 1978), especially if critical short-term
exposures and physiological response measurements are involved.

     Studies of air pollutants and other air-born toxicants have encouraged
the design of a wide array of controlled-exposure chambers covering a spectrum
from very simple (Berry and Ripperton, 1963) to extremely sophisticated (Heck
et al.t 1978).  Berry (1970) categorized the various chamber designs into four
general groups:  1) small modified greenhouses; 2) simple plastic enclosures for
use in greenhouse or laboratory; 3) modified growth chambers; and 4) plastic
chambers designed to fit in and utilize the environmental control of a growth
chamber.  The first two groups may utilize only natural light while the last
two require artificial light.  Examples of the various groups can be found in
Adams (1961), Berry and Ripperton (1963), Berry (1970), Cantwell (1968),
Costonis (1968), Heck et al. (1968), Heck et al. (1978), Hill (1967), Hitchcock
et al. (1963), Katz et al. (1939), Lockyer et al. (1976), Menser and Heggestad
(1964), Thomas et al. (1943), McLaughlin"et al•, Heagle and Philbeck (1979),
and Zimmerman and Hitchcock  (1956).  To Berry's list (Berry 1970) may be added
a fifth group which includes outdoor, open topped chambers for studying ambient
air pollutants under near natural conditions  (Heagle et al > , 1973).
                                      10

-------
     Heagle and Philbeck (1979) discussed various requirements of exposure cham-
bers used in studies of plants and air pollutants.  They concluded that a
chamber should have a continuous flow, single pass air stream containing the
desired pollutant.  The chamber walls should be inert to the pollutant and as
non-adsorptive of the pollutant as possible.  For plants, light transmitting
qualities of the chamber walls must be carefully considered if external lighting
is used.  Depending on the type of study, temperature and relative humidity
conditions may or may not be critically controlled and the level at which these
two conditions are to be maintained will govern the type and/or quality of
materials and equipment used within the chamber.  The most critical character-
istic of any chamber is the stability and homogeneity of the pollutant concen-
tration in space and time.  The mode of introducing the pollutant must be
stable over time and the movement of the air stream must not create eddies or
dead spots within the chamber.  Turbulent rather than laminar air flow is
generally desirable.

     For our experimental purposes, a reasonably large capacity, low cost, low
maintenance chamber was needed to study the long-term (2-4 months)  effects of
sulfur dioxide on developmental rates of grasshoppers and decomposition rates of
plant litter.  Internal temperature, humidity, and light controls were not
required since the chamber would be used in externally controlled environments.
However, the chamber needed to satisfy most of Heagle and Philbeck's (1979)
conditions.

                               CHAMBER DESIGN

     The chamber  (Figure 2.1) was constructed completely of 0.64 cm (1/tt")
thick plexiglass to allow use of ambient light conditions.  Since racks of
grasshopper rearing containers were to be used, the side-opening double doors
were made large for easy access to the chamber.  Weatherstripping was used to
seal around doors.  Air movement through the chamber was accomplished with a
push-pull system using an inlet and an exhaust fan.  The inlet fan air movement
capacity was rated at 25 percent of the exhaust fan (1.7 m3 • min"1 = 60 cfm).
This system created a negative internal pressure to prevent leakage.  Fans
were simple squirrel-cage types (Dayton Blowers, Dayton Electric Mfg. Co.,
Chicago).  The shroud on the inlet fan was removed to produce a symmetrical
dispersion  of S02-air mixture.  The S02 was introduced directly into the
incoming air stream as it entered the inlet fan.  To maximize the uniformity of
airflow through the chamber to the exhaust end, the inlet orifice of the exhaust
fan was directed to the downwind end of the chamber.  Sulfur dioxide concentra-
tions were measured through access holes drilled in the chamber top at three
points downwind.  At each point, holes were positioned to allow SC>2 measurement
with a stainless steel probe at numerous points in a cross-sectional plane.
Point measurements of 862 concentrations were made with a flame photometric
sulfur gas analyzer (Meloy Laboratories Inc., Model SA-160).  During the actual
studies, S02 concentrations were monitored by a chemical absorption technique
(using pararosanaline dye) which gave average concentrations over time (CFR,
1975).
                                      11

-------
           Inlet Fan with
            shroud removed
            (15 cfm rating )
                                                           Mounting Brackets
Exhaust Fan    u
 (60 cfm ratingL—!
Figure 2.1.    Diagram of  S02  exposure chamber.   A)  top view,  B) front view,
               Arrows  indicate air flow.
     Since our  objective  for  constructing the chamber was long-term exposure
capabilities, a low-cost,  low-maintenance source of S02 gas was needed.  A
small lecture bottle  of liquid  S02  proved quite adequate.  The gas was in-
jected into  the inlet fan air stream with the delivery system diagramed in
Figure  2.2.  Because the metering  valve was very sensitive to changes in
line pressure as  a result of  temperature changes on the S02 lecture bottle,
the bottle was  kept in a  refrigerated ice bath to keep temperature fluctua-
tions to a minimum.   The  ball valve was used to shut off gas flow without
affecting the metering valve  settings once a desired S02 delivery rate was
established.  A spring-loaded solenoid was installed on the ball valve handle
to prevent S02  buildup in the chamber in the event of an electrical power
failure.

                            OPERATION EFFICIENCY

     Air turnover in  the  chamber was calculated to be once every 1 to 2 min-
utes which produced an approximate  linear velocity of 0.46 to 0.91 m •  min~
                                       12

-------
                       All delivery lines
                       are 1/8" OD stainless
                       steel tubing.
                                             Nupro fine metering
                                                valve (stainless)
                                               Nupro Inline filter     c^.ffl2
                                                (7 micron, stainless)   bource
                 To inlet fan
                  orifice
                                                               Power
                                                               "Source
 Figure  2.2.     Schematic  of control panel.


 (1.5-3.0 ft  • min"1).  Air  flow rates were altered by either altering  the  inlet
 or exhaust fan  orifices or  changing either fan size.  The exposure system  as
 constructed was capable of  producing relatively stable S02 concentrations
 between 5 and 100 pphm although the lower and upper limits were not determined.

      Because the weatherstripping  used to seal the doors did not make  an
 absolute seal,  there was  slight variation of S02 concentrations both laterally
 and longitudinally.  At an  exhaust concentration of 20 pphm there was  a 3
 to 5 pphm longitudinal gradient with the  greatest decrease being from  the
 inlet fan to the hinge of the first door.   This upwind 30% of the chamber was
 considered as a dilution-mixing zone and  was not used for experimental pur-
 poses.   From the first door to  the exhaust fan the S02 gradient was less than
 2  pphm.  The variation (ma^min)  of  S02  concentration at a given cross-section^
 al plane was less than ±18 percent  of  the  mean concentration for that plane
 This was true for three different  concentration settings - 20,  17  and 8 5
 pphm mean concentration at the  exhaust  fan inlet.   The variation of S02 concen-
 tration  at  the exhaust fan inlet over time was  quite small - less than 1 pphm
 over long term intervals (up to  2 months)  and  less  than 0.5 pphm over short
 intervals (24 hours).

                                  CONCLUSIONS

      The controlled  exposure chamber herein  described  has  proven to be ade-
 quate for studies  involving long-term S02  effects on organisms  such as grass-
hoppers  and micro-organisms  involved in plant  litter decomposition.   It
satisfied most of  the  basic  conditions discussed by  Heagle  and  Philbeck
 (1979).   Its  utility could be  increased by use within  an environmentally
controlled greenhouse.   It is  comparatively simple and  inexpensive  to con-
struct and maintain.
                                      13

-------
                                 REFERENCES

Adams, D. F.  1961.  An Air Pollution Phytotron.   J.  Air Pollut.  Control
     Assoc., 11:470-476.

Berry, C. R.  1970.  A Plant Fumigation Chamber Suitable for Forestry Studies.
     Phytopathology, 60(11):1613-1615.

Berry, C. R., and L. A. Ripperton.  1963.   Ozone,  A Possible Cause of White
     Pine Emergence Tipburn.   Phytopathology,  53:552-557.

Cantwell, A. M.  1968.  Effect of Temperature  on Response of Plants to Ozone
     as Conducted in a Specially Designed  Plant Fumigation Chamber.  Plant
     Dis. Reptr., 52;957-960,

Code of Federal Regulations (Supplement to the Federal Register).  Title  40 -
     Protection of Environment, Part 50.11 July 1, 1975.  7 pp.

Costonis, A. C.  1968.  The Relationships  of Ozone, LophodeTm-iim  pinastri.
     and Pullularn-a pullulans to Needle Blight of Eastern White Pine.  Ph.D.
     Thesis, Cornell University, Ithaca, New York.  167 p.

Heagle, A.  S., D. E. Body, and W. W. Heck.  1973.   An Open-top Chamber to
     Assess the Impact of Air Pollution on Plants.  J. Environ. Quality,
     2(3):365-368.

Heagle, A.  S., and R. B. Philbeck.  1979.   Exposure Techniques, In:  W. W.
     Heck,  S. V. Krupa, and S. N. Linzon (eds.) Metholodology for the Assess-
     ment of Air Pollution Effects on Vegetation.   Air Pollution  Control
     Association, Pittsburg,  Pa.  pp. 6-1  to 6-19.

Heck, W. W., J. A. Dunning, and H. Johnson. 1968.  Design of a Simple Plant
     Exposure Chamber.  USDHEW Nat. Center Air Pollution Control  Pub. APTD-
     68-6 24 p.

Heck, W. W., R. B. Philbeck,  and J. A. Dunning.  1978.  A Continuous Stirred
     Tank Reactor (CSTR) System for Exposing Plants to Gaseous Air Contam-
     inants:  Principles, Specifications,  Construction and Operation. Agricul-
     tural  Research Service,  U. S. Dept. Agriculture,  ARS-S-181 32 p.

Hill, A. C.  1967.  A Special Purpose Plant Environmental Chamber for Air
     Pollution Studies.  J. Air Pollut. Control Assoc., 17(11):743-748,

Hitchcock, A. E., P- W. Zimmerman, and R.  R. Coe.   1963.  The Effect of
     Fluorides on Milo Maize (Sorghum sp.) Contrib. Boyce Thompson Ins!;.,
     22:175-206.

Katz, M., A. W. McCallum, G.  A. Ledingham, and A.  E.  Harris.  1939.  Des-
     cription of Plots and Apparatus used  in Experimental Investigations, In:
     Effect of Sulphur Dioxide on Vegetation.   Nat. Res. Council  Can.  No.
     815, Ottawa,  pp. 207-217.
                                     14

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Lockyer, D. R., D. W. Cowling,  and L.  H.  P.  Jones.   1976.  A System for
     Exposing Plants to Atmospheres Containing  Low  Concentrations  of  Sulphur
     Dioxide.  J. Exper. Bot.,  27(98):397-409.
McLaughlin,  S. B., V. J. Schorn, and H. C. Jones.   1979.   A Programmable
     Exposure  System for Kinetic Dose-response  Studies with Air Pollutants.
     J. Air  Pollut.  Control Assoc., 26(2):132-135.

Menser, H. A., and H. E. Heggestad.  1964.  A Facility for Ozone Fumigation
     of Plant Materials.  Crop. Sci.,  4:103-105.

Thomas, M. D., R. H. Hendricks, J. 0.  Ivie,  and G.  R.  Hill.  1943.  An In-
     stallation  of Large Sand-culture Beds Surmounted  by  Individual Air-
     conditioned Greenhouses.  Plant Physiol.,  18:334-344.

Zimmerman, P.  W., and A. E. Hitchcock.  1956.   Susceptibility  of Plants  to
     Hydrofluoric Acid  and Sulfur Dioxide Gases.   Contrib. Boyce Thompson
     Inst.,  18:263-279.
                                     15

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                                  SECTION 3

              A SYSTEM FOR MEASURING FOLIAR EXCHANGE RATES UNDER
                     ENVIRONMENTALLY CONTROLLED CONDITIONS

             S. R. Bennett, J. L. Dodd, W. S. Ferguson, C. J. Bleak,
                         G. L. Thor, and W. K. Lauenroth
                                   ABSTRACT

               A relatively Inexpensive physiological activity and
          diagnostic chamber designed to measure foliar exchange
          rates of S02, H20, and C0£ in grass leaves is described.
          The system consists of gas synthesis, cuvette, linkage,
          gas flow control and monitoring elements.  Equations for
          calculating gas flux rates are included.
                                 INTRODUCTION

     Investigations of the effects of gaseous air pollutants on plants take
many forms (Heck et- al., 1979).  Some research objectives are satisfied by
measurements of frequency of plant injury or percentage of foliar necrosis
while other research objectives require measurement of physiological changes
in response to particular pollutant exposure regimes (Tingey et al., 1979).
The latter approach is particularly suited to investigations of pollutant
mediated plant responses on a short term basis, or when exposure to low
concentrations of known toxic agents is not reflected in visible injury.

     The deleterious effects of S02 on vegetation have been widely documented
since its recognition as a chronic gaseous pollutant in industrialized areas-
(Ziegler, 1975).  Despite considerable research, anomalous physiological re-
sponses to S02 exposures not resulting in foliar injury and variable species
sensitivity to similar S02 concentrations remain unexplained (Thor, 1980).
The purpose of this paper is to describe a relatively inexpensive experimental
system designed to monitor foliar exchange rates of C02 and water vapor under
a range of controlled S02, relative humidity, and temperature conditions.

     The system described below was used to expose grass leaves to S02 con-
centrations between 10 and 100 pphm, relative humidity between 4.0 and 75.0
percent and temperatures between 5 and 28°C.  The apparatus consisted of a com-
pressed air supply which provided the carrier airstream through the system, a
gas synthesis subsystem, a multileaf cuvette, instrumentation to measure C02
S02, dew point, temperature and quantum irradiance, a data acquisition subsystem,

                                      16

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linkage, and control points for gas flow regulation.  This system is the type
of experimental apparatus termed "a physiological activity and diagnostic
chamber" by Bennett (1979).  It is similar in principle to the system described
by Winner and Mooney (1980).

                             MATERIALS AND METHODS

Experimental Cuvette

     Following a design similar to one described by Williams and Kemp (1978)
and Detling et al. (1979), a circular Plexiglass leaf cuvette 16.4 cm in
diameter was constructed.  The device consisted of two fitted sections,
forming a 3.6- cm high chamber surrounded by upper and lower water jackets
for temperature regulation (Figure  3.1).  The water jackets were connected
to a circulating bath equipped with flow rate and temperature control.   A
magnetic stir bar in the lower chamber of the cuvette insured a homogenous
air mixture and reduced boundary layer resistance.  Boundary layer resistances
were 0.2 ± 0.1 s • cm"1 in a system of similar design and operational protocol
(Kemp, 1977).

     The cuvette was sealed by compressing a narrow bead of nontoxic sealing
compound (Mortite) between the two cuvette sections.  Grass leaves were  en-
closed between the fitted sections and rested on fine nylon line strung  above
the stir bar.  In addition to providing an airtight seal, the mortite func-
tioned as a protective cushion which completely surrounded the leaves.   Air
temperature within the cuvette was continuously monitored with a shaded  YSI
thermistor (Model 421).  Leaf temperatures were not measured but were assumed
to be equivalent to air temperatures within the cuvette.  Detling (unpublished)
tested a cuvette of similar design and operational protocol and found leaf
temperatures of well-watered plants to be within 1°C of cuvette air tempera-
tures.  Irradiance was supplied by a 1,000 watt Westinghouse Ceramalux high
pressure sodium lamp suspended on a pulley directly above the cuvette.
Quantum irradiance maintained at 1250-1350 \iE m~2 s"1 was measured with  a LI-
170 Quantum sensor photometer and was controlled by varying the distance
between lamp and cuvette.  A water screen placed directly beneath the sodium
lamp aided in reducing heat transfer to the cuvette.

Gas Synthesis

     Initially air was obtained from a central compressor in the laboratory
and was carried through the gas exchange system in heavy wall 1/4" Tygon
tubing.  This was supplemented where necessary with short lengths of 1/4"
stainless steel,  1/it"  copper and I/it';)' glass tubing.   Carbon dioxide was  elim-
inated by passing the  airstream through a concentrated potassium hydroxide trap,
and molecular sieves  (Matheson Model 460 Gas  Purifier) placed in series  removed
oil and water contamination.  Last, a column of desiccant and a column of
ascarite (NaOH, A.  H.  Thomas Company)  placed in series removed remaining
traces of water vapor  and C02, respectively (Figure  3.2).  The air obtained
from the laboratory compressor contained variable amounts of C02 and moisture
and was later replaced with medical grade reconstituted air.  The cylinders
of reconstituted air provided an air supply which was uniformly dry and  C02
free.   Utilization of  reconstituted air also eliminated the need for extensive

                                     17

-------




0.3 cm-

Outlet ^
water — £__
port
0 3cm
Outlet f-l
gas port ^

.0 cm<-. ,

Outlet 	
water — t^,







KW
*M*






fffif
«A*

Tl ~^ rm
1 7 n r n\



i
| 2.2 cm I


.0 cm
\
i (
I.S^cm ^ Magnetic stir bar j
I 2.2 cm 1
' i
i






WM
VA»






AW>
\W






llnl*n» IMtAV i^/\bA4
~2- lnle* water port


Upper cuvette half
-^Compression
flanges
^3— Inlet gas port
	 Lower cuvette
half
_j3 — Inlet water port
Water jacket
             Cuvette  volume   760 cm3       Water jacket (single) volume: 470 cm3
                 Outlet water port
                     Inlet gas port




          Outlet water port
                                                              r—/—Inlet water port
Nylon line
                                                                  Inlet water  port
Figure   3.1.    Experimental  plexiglass  cuvette design.
                                             18

-------
              Bath
               Humidifier
   Circulating
     Bath
                       t
S02
Analyzer



J





i


H
i
                                  Dew-point
                                  hygrometer
                                                 -O-JL
-------
C02  scrubbing, and  the potassium hydroxide  trap was eventually removed,
making  the system less labor  intensive.

     The scrubbed airstream was bubbled  through a stainless steel humidifier
immersed in a temperature controlled bath.  The humidifier consisted of a
1500-ml capacity water reservoir and a baffled air space packed with sufficient
coarse  steel mesh to prevent  aspiration  of water into air lines during opera-
tion.  This simple  humidification system permitted stable dewpoints to be
achieved and manipulated during experimentation.

     Carbon dioxide prepared  at 4.0 percent in air was  introduced into the
humidified airstream with a fine metering valve  (NUPRO  B-45G 0.031" orifice).
The  fine metering valve permitted minute adjustments in C02 flow rate and
allowed for the establishment of reproducible C02 concentrations  (ca. 330 ppm).

     Sulfur dioxide prepared  at 50 ppm in N2 was introduced downstream from
CO2 with a stainless steel fine metering valve (NUPRO-SS-45G 0.031" orifice)
in a manner similar to that described above for C02.  Concentrations of S02
between 10 and 100 pphm could be achieved within minutes and maintained in
the  system for several hours.

Gas Analysis

     Relative humidity in the airstream  was calculated  from the cuvette air
temperature and the dewpoint, continuously measured with a thermoelectric
hygrometer (Cambridge Systems Model 880-C1)-

     Concentrations of C02 were continuously monitored  with an infrared gas
analyzer (IRGA, Beckman Instrument Company).  Calibration of the IRGA required
manually by-passing the cuvette so that  the airstreams  entering the sample
and reference cells were identical.  In  this mode, independently measured C02
calibration gases were introduced, either to calibrate  the instrument or to
establish a particular C02 concentration in the airstream.

     A flame photometric sulfur gas analyzer (Meloy Laboratories Inc.  Model
SA-160) was used to continuously measure S02 levels in  the airstream.   The
sulfur analyzer was calibrated with a permeation tube calibration system
(Metronics Associates Inc., Dyna-calibration Model 330).

     A permanent record of C02 and S02 concentrations and dewpoint temperatures
was made for cuvette inlet and outlet airstreams for each experiment on a
multichannel strip  chart recorder (Texas Instruments Inc. Model FMW SE-60
Multiriter).

Direction of  Flow

     The fully reconstituted  airstream was  divided into reference and  sample
lines,  each consisting of a valve, a flow meter, a desiccant, and a filter
before entering an IRGA cell  (Figure   3.2).  The sample airstream was
directed through a bank of solenoid valves  and the leaf cuvette before entering
the IRGA sample cell.  After  exiting the IRGA, the sample airstream passed
through an additional flow meter which was  used to detect leakage from the


                                      20

-------
cuvette.  The reference airstream was directed into an exhaust port after
exiting the IRGA reference cell.

     Two additional air lines (Figure  3.2, A and B), diverted portions of
the reference and sample airstreams to a 3-way valve (Whitey B-43XF4 0.187"
orifice).  This valve was used to manually direct the airstreams alternately
through both the sulfur analyzer and dewpoint hygrometer.  Changes in the
cuvette environment were detected by alternate measurement and comparison of
the two airstreams.

     Just prior to the entry point for S02, another air line (Figure  3.2, C)
diverted a portion of the airstream to the bank of solenoid valves located
just above the cuvette.  The air in this line remained S02-free, but in all
other respects was identical with the fully reconstituted airstream.  The
solenoid valves permitted instantaneous routing of either the sample or SC-2-
free airstream through the cuvette, automatically diverting the unused air-
stream to an exhaust port.  Routing SC^-free air through the cuvette allowed
S02 concentrations to be achieved and stablized in the sample and reference
lines without disrupting the environmental equilibrium of the cuvette.  This
arrangement also made it possible to instantaneously expose the cuvette to
stable, predetermined levels of S02 without first isolating the cuvette from
the system.  Flow rate in the S02-free line was established prior to full
reconstitution of the airstream and continued unchanged for the duration of
each experiment.

Regulation of Flow

     Flow rates in the gas exchange system were regulated at three principle
points.  The flow rate of scrubbed air entering the system was controlled by
a fine metering valve (Nupro B-4MG 0.055" orifice) located just above the hu-
midifier (Figure  3.2).  Flow rates in the reference and sample lines could
be adjusted during operation with individual valves located at the beginning
of each line.  Generally, a flow rate (1.0 1 m"1 1.5 1 m"1) sufficient to
maintain a 1500-2500 pphm C02 differential between the sample and reference
lines was established at the beginning of an experiment and continued unchanged
for its duration.  The fine metering valve controlling the supply of scrubbed
air could not be changed during an experiment since any change in flow rate
at this point in the system would disrupt the established ratio of gases.

Calculations

     Rates of photosynthesis and transpiration uptake were represented by the
following gas flux equations (Winner and Mooney, 1980).

                              J  = A  FA'1 t
                               x    x

where

     J  = flux rate for any gas (mass area"1 time""1)
     A  = change in gas concentration due to experimental leaf tissue (yl I"1)

     F  = air flow rate (1 nT1)

                                      21

-------
     A  =  area  of  experimental  leaf  tissue  (dm2)


     t  =60 min



     Appropriate constants  for  local temperature.and  atmospheric pressure were

 multiplied into the  above calculation.



     When  A  measurements were  made  for  C02,  and  water vapor,
           2C



     Jx  -  V Jt>


 thus



     J  =  J  =  net photosynthesis  (yg C02 dm"2 hr"1)


         =  J  =  transpiration  (g F^O  dm-2 hr"-1)



     Stomatal conductance values for water vapor  (C ) and  S02  (C ) were calcu-

 lated  as                                                        s



     C  =  1/R
       w      w


     R  =  (H. - H )  • p  • 3.6 x 105
       w     i	a	


                     Jt



     R  =  resistance to water vapor  (s • cm"1)
       w


     H. =  specific humidity of  air in substomatal chamber

     H =  specific humidity of  air outside leaf
       3.
     p  = air density


     J  = transpiration


     3.6 x 105 = conversion factor for units
and
     C  = C  • D
      s    w    s

               D
                w
where
     C  = conductance for water vapor
     ,w
     D  = diffusivity coefficient for water vapor  (0.2475)
      w
     D  = diffusivity coefficient for S02  (0.1313)
      s
     Flux of SC>2 through the stomates  (yg  • cm~2  • s) was then calculated as
     F  = S  - S,
      s    a	]

           R
            s
                                      22

-------
where

     R  = 1
      S   C~
           s
     SE = S02 concentration in air around leaf (exit concentration)

     Si = S02 concentration in substomatal chamber (assumed to be 0)

Operational Protocol and System Performance

     The system was applied to attached leaves of several species of grass
plants according to the following general procedure:

     1.   Preliminary calibration and adjustments were made on all gas
          synthesizing, environmental control, and monitoring equipment.

     2.   Two or three healthy leaves of each plant were sealed into the
          cuvette.

     3.   Final adjustments were made on all control points to attain
          precise environmental conditions prescribed for a given trial.

     4.   The system was then allowed to equilibrate until inlet and outlet
          dewpoints, C02 uptake rates, and cuvette air temperatures were
          stable for at least 30 min.  The stable period was considered
          the control.

     5.   Simultaneous with Step 4, S02 was introduced into an airstream
          bypassing but otherwise identical to that flowing into the
          cuvette.  Sulfur dioxide concentration in the airstream was set
          to a specified level.

     6.   At the end of the control period the airstream containing S02
          was routed into the cuvette and the SC>2-free airstream was
          directed to an exhaust manifold via a solenoid switching mechanism.

     7.   Exposure of the leaves to S02 was continued until CC>2 and H20
          flux rates attained an apparent stable rate for at least 30
          minutes.  In most trials the rates stabilized within about 15
          to 20 minutes and the trial was terminated after 1 hr  of ex-
          posure.

     Results of two representative S02 exposure trials are shown in Table
3.1.  In trial A,  C02 flux and transpiration rates decreased to a stable
rate within 10 min.  Trial B leaves exhibited lower control photosynthetic
rates and higher transpiration rates and did not stabilize until about 30
min  into the exposure period.  Stomatal flux rates of S02, being based
on water vapor conductance rates and cuvette outlet concentrations of S02,
closely paralleled rate dynamics of transpiration because the outlet S02
concentrations were reasonably stable through these runs.
                                      23

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TABLE  3.1.  GAS EXCHANGE DYNAMICS  AND ENVIRONMENTAL  CONDITIONS  FOR TWO EXAMPLE TRIALS (A AND B) UTILIZING
             ATTACHED LEAVES OF HYDROPONICALLY GROWN  WESTERN WHEATGRASS PLANTS
Control*
Trial
S02 concentration (pphm X 10"1)
cuvette inlet
cuvette outlet
Air temperature (C°)
Ir radiance (yE • dm~2 • s"1)
K> Absolute humidity (g H20 • m"3 air)
cuvette inlet
cuvette outlet
C02 concentration (ppm X 10"1)
cuvette inlet
cuvette outlet
Flow rate (1 • min-1 X 102)
Leaf area (cm2 X 10)
Atmospheric pressure (mb X 10"1)
C02 flux (mg C02 • dm"2 • hr"1)
Transpiration
(g H20 • dnT2 - hr"1 X 10)
Stomatal flux of S02
(ng S02 • cm"2 • s-1 X 102)
A
0
0
23.9
12.5
8.5
11.0
35.2
32.9
95.0
90.7
85.4
22.0
18.5
0
B
0
0
23.9
12.5
7.2
11.6
34.9
32.5
95.0
101.8
85.3
20.5
24.8
0
A
10.7
8.9
23.9
12.5
8.4
11.0
35.2
33.3
96.0
90.7
85.4
18.4
16.3
41.0
10
B
10.7
7.6
23.9
12.5
6.9
11.5
34.9
32.7
95.0
101.8
85.3
18.8
25.4
56.8
Elapsed time (min) from initiation
A
10.7
9.0
23.9
12.5
8.4
11.0
35.2
33.3
96.0
90.7
85.4
18.4
16.3
41.5
20
B
10.7
8.1
23.9
12.5
7.0
11.2
34.9
32.8
95.0
101.8
85.3
18.4
23.5
54.8
A
10.7
9.1
23.9
12.5
8.4
11.0
35.2
33.3
96.0
90.7
85.4
18.4
16.3
42.0
30
B
10.7
8.2
23.9
12.5
7.0
11.1
34.9
32.8
95.0
101.8
85.3
17.9
23.5
55.7
of S02 exposure
A
10.7
9.3
23.9
12.5
8.4
11.0
35.2
33.3
96.0
90.7
85.4
18.4
16.3
43.0
60
B
10.7
8.4
23.9
12.5
7.1
11.2
34.9
32.8
95.0
101.8
85.3
17.9
23.0
55.8
A
10.9
9.5
23.9
12.5
8.4
11.0
35.2
33.3
96.0
90.7
85.4
18.4
15.9
42.8
120
B
10.7
8.8
23.9
12.5
7.2
11.2
34.9
32.8
95.Q
101.8
85.3
17.5
22.2
55.9
 Control data is from a 30 to 60 minute interval immediately preceding initiation of S02 exposure when all monitored parameters were stable.

-------
     Certain problems were encountered in utilizing this system in nearly 200
trials.  The major problem was our inability to monitor dewpoint of the inlet
and outlet airstreams precisely.  The dewpoint hygrometer utilized is capable
of determinations to the nearest 0.5°C.  Consequently,  our estimates of
transpiration and stomatal flux of S02 were frequently variable and only of
general value.  The strong points of the system are that it permits fairly
precise measurement of C02 exchange rates in grass leaves under a range of
environmental conditions and is relatively inexpensive.

                                   CONCLUSIONS

     The gas exchange system described proved to be a relatively inexpensive
but effective means to measure effects of low-level, short-duration S02 ex-
posure on sulfur uptake, net photosynthesis, and transpiration in western
wheatgrass leaves.  Although S02 and H20 exchange rates could only be measured
rather crudely the performance characteristics of the system were generally
very good.  A rapid response time permitted several short-duration experi-
ments at varying conditions to be conducted within a single 8-10 hr period.
Although the system was incapable of measuring fluxes of C02, S02 and water
vapor at the level of precision achieved by Winner and Mooney (1980) with
their more sophisticated system, we conclude this system has utility in
studies where objectives require less precision and where fiscal resources
are more limited.

                                  REFERENCES

Detling, J. K., M. I. Dyer, and D. T. Winn.  1979.  Net Photosynthesis, Root
     Respiration, and Regrowth of BouteZoua gracilis Following Simulated Gra-
     zing.  Oecologia, 41:127-134.

Bennett, J. H.  1979.  Foliar Exchange of Gases.  In:  Methodology for Assess-
     ment of Air Pollution Effects, W. W. Heck, S. V. Krupa, and S. N.
     Linzon, eds.  Air Pollution Control Association.  Ch. 7.

Heck, W. W., S. V. Krupa, and S. N. Linzon, eds.  1979.  Methodology for the
     Assessment of Air Pollution Effects on Vegetation.  Air Pollution Control
     Association.

Kemp, P. R.  1977.  Niche Divergence Between Agropyron smithii., C3, and
     Bouteloua graoil-is, C^:  A Study of the Role of Differing Photosynthetic
     Pathways in the Shortgrass Prairie Ecosystem.  Ph.D. Dissertation.
     Washington State University, Pullman, Washington.

Thor, G. L.  1980.  Photosynthesis in Western Wheatgrass Exposed to Chronic
     S02 Air Pollution.  M.S. Thesis, Colorado State Univ., Ft. Collins.  71
     pp.

Tingey, D. T., R. G. Wilhour, and 0. C. Taylor.  1979.   The Measurement of
     Plant Responses.  In:  Methodology for Assessment of Air Pollution
     Effects, W. W. Heck, S. V. Krupa, and S. M. Linzon, eds.  Air Pollution
     Control Association.  Ch. 7.
                                      25

-------
Williams, G. J., Ill, and P. R. Kemp.   1978.   Simultaneous Measurement of Leaf
     and Root Gas Exchange of Shortgrass Priarie Species.   Bot.  Gaz.,  139:ISO-
     IS?.

Winner, W. E., and H. A. Mooney.  1980.   Ecology of  S02 Resistance:  I.
     Effects of Fumigations on Gas Exchange of Deciduous and Evergreen Shrubs.
     Oecologia.

Ziegler, I.  1975.  The Effects of S02  Pollution on  Plant  Metabolism.   Residue
     Rev., 56:79-105.
                                     26

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                EFFECTS OF CHRONIC S02 EXPOSURE ON ENERGY FLOW
                      AND NUTRIENT CYCLING IN GRASSLANDS
                                   SECTION 4

                   THE EFFECT OF S02 ON 14C TRANSLOCATION IN
                              WESTERN WHEATGRASS

               D. G. Milchunas, W. K. Lauenroth, and J. L. Dodd
                                   ABSTRACT

               Translocation of photoassimilated IttC02 by individual
          source leaves of Agropyron smithii- Rybd. was stimulated by
          exposure of the plants on ZAPS I High plot.  Labeled leaves
          exposed to S02 exported an average of 12 percent more carbon
          than control leaves.  This was in response to an increased
          sink demand of expanding leaves.  The relative concentration
          and relative partitioning of 14C in developing leaves was
          177 and 153 percent greater, respectively, in plants on the
          S02 treatment than in Control plants.  Belowground lltC
          concentrations were greater in S02 exposed plants only on
          the early growing season sampling date.  Increased rhizome
            C relative concentration suggests greater sink demand
          in reproductive as well as vegetatively growing components.
          a comparison is made between productivity, photosynthetic
          and ^ C partitioning responses in monitoring the subtle
          effects of low-level S02 exposure.
                                  INTRODUCTION

     The partitioning of photoassimilated carbon among various plant organs is
an important aspect in the functioning of a plant as an integrated system.
Translocation processes, and the maintenance of carbon balance, are subject to
regulation involving both positive and negative feedback mechanisms (Geiger,
1979).  The export of carbon from a source leaf is a function of the availa-
bility of sucrose and other mobile molecules, and the demand for these assimi-
lates in other locations.

     Plant nutrient levels can affect translocation independent of carbon
assimilation rates.  Increased levels of free-space potassium did not increase
net carbon fixation but increased the proportion of fixed carbon which was
exported (Geiger, 1979).  Similar affects for levels of inorganic phosphorus and
nitrogen were suggested by the observation that deficiences of phosphorus and
nitrogen caused a decrease in the efflux, into solutions, of assimilated carbon
from the mesophyll of beet leaves (Kamanina and Anisimov, 1977).


                                      27

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      Sulfur  dioxide  exposure has been  shown  to  affect photosynthesis,  amino
 acid production,  and carbohydrate metabolism in plants  (Ziegler,  1975).
 Large quantities  of  sulfur accumulate  in plants exposed  to  S02  depending  on
 the concentration and duration of exposure and  the  environmental  conditions
 during exposure  (Lauenroth et al. , 1979).  Short-term exposure  to S02  has
 been shown to  inhibit phloem translocation more than photosynthesis  (Teh  and
 Swanson,  1977).   Exposure of plants to  S02 then, may affect  translocation
 directly  as  well  as  indirectly by its  impact on assimilate  supply/sink de-
 mand.   In this study we examined the effect  of  a controlled  level of S02  expo-
 sure through the  growing season on translocation of 14C  in Agropyron smithii
 Rybd.  in  a native Montana grassland ecosystem.  Agropyron smithii was  dominant
 within the study  area and is an important forage species throughout the
 northern  Great Plains.

                            MATERIALS AND METHODS

      Twelve  western  wheatgrass (Agropyron smithii) plants, with an equal
 number of  fully expanded leaves, were chosen on the Control  and High S02
 treatment  plots for  labeling with lttC02.  Three leaf age classes  were  labeled.
 Leaf numbers were  assigned from lowest  to highest on the plant; i.e. the
 oldest leaf  was considered leaf number  one.  Leaf numbers three,  four, or
 five were labeled on June 18 and 26, and leaf numbers five,  six,  or seven
 on July 15 and August 2 sampling dates.

      Individual leaves were placed in a cuvette, sealed with putty, and
 exposed to 14C02  O330 ppm)  of specific activity 3.7 x 107 Bq mmol"1 (1 mCi
 mmol"1 for 2 minutes  in full sunlight.  After 3 days the plants were collected
 and  separated  into the three leaf age classes,  the developing leaf, other
 aboveground leaves and stem, roots, and rhizomes.   Roots were sampled  to  a
 depth  of 10 cm.   In  a previous experiment on this study area, 62  percent  of
 the  belowground ^C was located in roots from the O-10 cm zone  (Coughenour
 et al,, 1979).   All  samples were oven dried  at  60°C to a constant  weight.

     The oven-dried  samples were enclosed in Whatman low as-h filter paper and
 compressed in  a pill  press to reduce their size.  The plant material was
wrapped in filter paper because grinding was impractical due to sample size
 and  static electricity problems.  Samples were  then combusted in  a Packard
 Instrument Co.  model  306 Tri-carb sample oxidizer which automatically absorbed
 the  lltC02 in Carbo-sorb II and placed it in a liquid scintillation vial with
Permafluor V scintillation cocktail.  Sample activities were counted on a
Nuclear-Chicago Mark II liquid scintillation system.

     The data  are expressed as relative concentrations or relative quantities
in each plant  component.  Relative concentration (CPM/mg of plant  tissue)
describes the  sink strengths while relative amounts (CPM/total sample)  of
in each component directly addresses the movement of carbon.  Because it was
impossible to  collect the entire belowground biomass for each labeled plant,
discussions relating  to aboveground/belowground are based only upon the
concentration  data (CPM/mg dry wt) .  Aboveground data are presented on  both a
sink strength  and distribution basis.
                                      28

-------
     Two aspects of our experimental design need clarification for proper in-
terpretation of results.  First, we refer to leaf age class rather than leaf
age because both leaf age and the position of a leaf relative to carbon sinks
can influence translocation (Wardlaw, 1968; Mor and Halevy, 1979).  However,
in an erect culm grass like Agvopyron smithii,, leaf position is a function of
leaf age.  Therefore, in this study leaf age and leaf position are not separ-
able yet neither are they a source of possible interaction between plant
replicates (i.e., there is no possible age x position interaction).  Second,
leaf age classes remained constant for all dates.  Date effects can only be
attributed to overall plant phenology and the presence oi additional and
older leaves on the plant.

     Data were subjected to an analysis of variance using a modified split
plot design with subsampling.  The main plot was S02 treatment and the split
plot a 4 x 3 factorial of date by leaf.  Replicates were arranged in. randomized
block fashion.  Tukey's Q values were used to compute least significant
ranges (LSR) and identify significant differences between means (Sokal and
Rohlf, 1969).

                                    RESULTS

     Three days after exposure to  lkCC>2, labeled leaves contained a higher
concentration  (CPM/mg) and quantity  (CPM) of lkC than other aboveground plant
components regardless of date or SO2 treatment  (Table  4.1).  Sulfur dioxide
exposure significantly reduced the concentration  (P = 0.06) and total quantity
 (P = 0.01) of  14C remaining in labeled leaves indicating the presence of high
demand in other plant components.  Labeled leaves exposed to SO2 exported an
average of 12 percent more carbon  than the leaves of control plants.  Import
of  14C by mature unlabeled leaves  accounted for 0.5 percent of the total
aboveground lltC in  Control plants  and 1 percent in those exposed to SC^-
Other aboveground plant parts, excluding the developing leaf, accounted for
17 and 22 percent of the aboveground Il*C for the Control and S02 treated
plants, respectively.

     The concentration (P = 0.001) and total quantity (P = 0.05)  of 14C
remaining in labeled leaves was significantly influenced by the age class of
the labeled leaf.  Labeling the youngest, middle, and older fully expanded
leaf resulted in lt+C concentrations which represented 79, 83 and 92 percent
(LSR = 10) of the total aboveground concentration, respectively.   Total
quantities of 11+C retained in the labeled leaves showed the same pattern.
The three leaf age classes from young to old retained 67, 77,  and 84 percent
(LSR = 11) of the total above ground activity.  The large quantity exported
from younger leaves may be a function of their age or proximity to the devel-
oping leaf.

     In many cases the developing leaf was a strong carbon sink (Table 4.1).
The concentrations and quantities of iLfC in developing leaves were 1.5 and
1.7 times greater,  respectively, in S02 treated plants than control plants.
Young leaves rely upon translocated carbon until they develop sufficient
photosynthetic capacity to satisfy their needs.   Swanson et al. (1976),
Thrower (1962) and Fellows and Geiger (1974)  reported that peak demand for
carbon by developing leaves occurred when the leaf was approximately 25


                                     29

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TABLE  4.1.  CARBON-14  RELATIVE CONCENTRATION AND PARTITIONING IN AGROPYRON
             SMITEII EXPOSED ON THE ZAPS I HIGH PLOT.   VALUES ARE BASED ON
             MEANS FOR  PLANTS  HARVESTED 3 DAYS AFTER I4C02 ASSIMILATION
1J|C Mean Activity (%)
Date Treatment
June 18 Control




S02




June 26 Control




S02




July 15 Control




S02




August 2 Control




S02




Plant Part*
Leaf 3
Leaf 4
Leaf 5
Devl.Lf .
Other
Leaf 3
Leaf 4
Leaf 5
Devl.Lf.
Other
Leaf 3
Leaf 4
Leaf 5
Devl.Lf.
Other
Leaf 3
Leaf 4
Leaf 5
Devl.Lf.
Other
Leaf 5
Leaf 6
Leaf 7
Devl.Lf.
Other
Leaf 5
Leaf 6
Leaf 7
Devl.Lf.
Other
Leaf 5
Leaf 6
Leaf 7
Devl.Lf.
Other
Leaf 5
Leaf 6
Leaf 7
Devl.Lf.
Other
Labeled Old Leaf
CPM/mg CPU
97.0
0.6
0.4
0.1
1.1
89.0
1.1
0.8
6.8
2.3
97.6
0.2
0.5
1.2
0.5
91.3
1.6
0.8
2.9
3.4
95.2
1.1
0.3
3.2
0.2
91.1
2.8
0.9
2.8
2.4
94.0
0.6
0.3
4.7
0.5
84.3
2.8
0.9
11.0
0.9
95.4
0.8
0.6
3.0
1.0
74.9
1.4
1.0
20.8
2.0
95.0
0.2
0.5
3.9
0.5
87.7
1.5
0.8
10.5
1.9
87.2
1.0
0.2
11.5
0.1
86.5
2.9
0.7
9.4
0.6
78.5
0.5
0.2
20.8
0.1
65.3
2.2
0.5
31.8
0.2
Labeled Middle Leaf
CPM/mg CPM
0.2
77.5
0.9
3.4
18.0
0.4
84.5
1.2
10.1
3.9
0.7
91.6
1.2
5.4
1.2
1.9
74.9
2.4
6.2
14.6
0.8
89.8
2.1
6.2
1.1
0.3
74.5
1.8
2.6
20.8
0.5
91.9
1.1
6.2
0.3
0.7
80.7
2.5
14.9
1.2
0.2
82.8
0.9
9.3
3.6
0.2
78.5
1.1
18.1
2.8
0.5
78.5
0.8
19.4
0.8
1.6
67.7
3.0
20.1
7.7
0.7
76.4
1.6
20.9
0.4
0.4
82.6
1.7
9.7
5.7
0.5
81.7
0.7
17.1
<0.1
0.5
64.7
1.6
32.9
0.3
Labeled Young Leaf
CPM/mg CPM
0.1
0.4
82.-0
8.7
9.1
0.2
0.3
64.1
13.4
22.1
0.3
0.9
82.8
8.5
7.5
0.5
0.3
64.3
8.2
26.9
0.2
0.4
90.1
5.7
3.6
0.6
1.5
88.8
3.2
5.9
0.1
0.7
90.7
7.6
0.8
0.4
0.9
73.0
10.0
15.7
<0.1
0.1
76.5
17.0
6.3
0.1
0.2
43.1
46.8
9.8
0.3
0.9
61.9
32.4
4.6
0.5
0.3
64.2
25.2
9.0
0.2
0.3
77.1
20.9
1.6
0.6
1.4
84.3
10.8
2.8
0.1
0.7
70.2
28.9
0.1
0.5
0.8
57.8
36.3
4.6
  Leaf counts are from bottom to top of plant.  The highest number represents the youngest
  fully expanded leaf. Devi. Lf.  refers to the new developing leaf.  Other refers to the
  stem and leaves other than the 3 top leaves and the developing leaf.
                                        30

-------
percent of its final  length.  We  investigated  the  possibility that the greater
  C activity in developing  leaves  on  the  SC>2 treatment was a function of leaf
size rather than a  treatment  effect.

     Mean weights and the distribution  of weights  for  the  developing leaves
between the Control and  the S02 treatment were very  similar (Figure  4.1).
These data were subjected to  the  same analysis of  variance model used to
examine 11+C partitioning and  no significant differences (P = 0.80)  were
observed in leaf weight between the Control and  S02  treatment.   Differences
in developmental stage were not significant for  any  three  or two way inter-
actions or for main effects with  the  exception of  date.  Weights of expanding
leaves by date were 20.8, 18.4, 15.4, and 10.1 (LSR  8.7) for June 18, 26,
July 15, and August 2, respectively.  This suggested a decline  in weight of
expanding leaves as the  season progressed rather than  an unequal distribution
of weights sampled.   Further, in  all  our  analyses  of variance,  date was a
significant factor  in date  x  treatment  interactions  rather than as  a main
effect.  The analysis of variance  for expanding  leaves indicated that although
weights declined as the  season progressed, they  remained uniform within a
date-between-treatments  or  labeled-leaf-age classes.   The  greater translocation
in plants on the S02  plots  was therefore  in response to S02 exposure and not
because of nonuniform sizes of developing leaves between treatments or labeled
leaf age classes.

     The balance between above- and belowground  sink strengths  was  modified by
the interactions between treatment and  date (P = 0.01)  and between  treatment
                    1	[	1	1	1	1	1
                    0-4  4-8  8-12 12-16 16-20 20-24 24-28 28-32 32-36 36-40
                                EXPANDING LEAF WEIGHTS Cmg)
Figure  4.1.   Weight distribution of expanding leaves of Agropyron smithii-
               plants on the Control (	) and S02  (	)  treatment.
                                      31

-------
 and leaf age class (P = 0.03).  Plants receiving SC>2 displayed significantly
 higher belowground 1IfC concentrations on June 18 both compared to  the Control
 plants and to other dates within the SC>2 treatment (Figure  4.2).  Above- to
 belowground lltC concentrations within the Control were not influenced by
 date.   The significant date and treatment effects can be attributed  to  the
 June 18 high rhizome -^C concentration in plants on the 502 treatment  (Table
  4.2).

      The age class of the labeled leaf influenced above- to belowground 11+C
 concentrations in plants on the S02 treatment but not in Control plants
 (Figure  4.3) .  Belowground 1LfC concentration on the SC>2 treatment became
 proportionately less when younger leaves higher on the grass culm were  labeled.
 This occurred in response to the younger and older leaves respective proximity
 to greater sink demand of the expanding leaves and the rhizomes of plants on
 the S02 treatment.   However, even in the presence of greater aboveground
 assimilate demand in plants on the 862 treatment, the concentrations of
 belowground 11+C between plants on the Control and 862 treatments were not
 different when the youngest leaves were labeled and were greater on  the S02
 treatment when the older leaves were labeled.
 o

 o
 u.
 c
 QJ
 O
 C
 o
 o

 O •£•
* c
~ 
 O)
 O
JD
            3
            o
            
            GO
                 lOOr
                  95
                  90
                 85
                            LSR
                            2 4
                      Control S02 Control S02
                        June 18    June 26
                               Control S02  Control S02
                                  July  15     Aug  2
Figure  4.2.
Aboveground  (Y////A )  to belowground (I    I)  relative  14C
concentrations  (CPM/mg)  for Control and S02  treatments by
date.  Use LSR2 for within date across treatment comparisons;
and LSR^ for within treatment across date  comparisons.
                                      32

-------
TABLE  4.2.  CARBON-14 RELATIVE CONCENTRATION IN BELOWGROUND COMPONENTS.
             BELOWGROUND PARTITIONING DATA IS NOT PRESENTED BECAUSE 100
             PERCENT OF THE BELOWGROUND BIOMASS WAS NOT SAMPLED

•^C Mean concentration (%)
Date Treatment
June 18 Control
S02
June 26 Control
S02
July 15 Control
S02
August 2 Control
S02
Plant Part
Root
Rhizome
Root
Rhizome
Root
Rhizome
Root
Rhizome
Root
Rhizome
Root
Rhizome
Root
Rhizome
Root
Rhizome
Labeled
Old Leaf
CPM/mg
0.9
0.6
9.2
17.5
1.4
2.3
4.1
3.3
1.6
1.7
3.9
3.2
1.1
4.2
3.9
6.7
Labeled
Middle Leaf
CPM/mg
0.9
5.2
3.0
11.9
3.4
2.7
4.2
2.7
2.7
3.5
2.3
1.0
3.9
4.3
10.3
Labeled
Young Leaf
CPM/mg
0.5
0.7
3.1
1.5
2.4
3.1
2.4
4.2
2.6
4.0
2.9
1.1
1.0
6.6
2.6
6.1

                                   DISCUSSION

     A stimulation in translocation of I4C from the labeled leaf in the
aboveground compartment was observed in Agropyron smithii exposed on the ZAPS
I High plot.  The increased translocation was in response to the greater sink
demand of developing leaves.  Export to the developing leaf was greatest from
the young fully expanded leaf nearest the sink.  The greater sink demand of
developing leaves in the plants exposed to S02 could be the result of more
rapid cell division and growth rates, or because a slower development of
photosynthetic capacity in  the developing leaves exposed to S02 requires
greater or longer carbon import from mature leaves before they are self
sufficient.  Increased translocation from mature leaves which are fixing less
carbon is possible because  sink demand can override the availability of
                                      33

-------
                100 r
         o>
         0
         c
         o
         o
         o
         0>
         >
         o
         jQ
         o
         I
        m
Figure   4-3.
              Control  S02  Control S02 Control S02
                 Old         Middle       Young
                                                                     1Lf
Aboveground (.V////A") to belowground ( |      |) relative  fC
concentrations (CPM/mg) for Control and SC>2 treatments when
the old, middle and young leaves were labeled.  Use LSR2 for
within leaf age class across treatment comparisons, LSR3 for
within treatment across leaf age class comparisons, and LSR6
for across treatment across leaf age class comparisons.
assimilate in regulating translocation  (Ho, 1979) .  It is first necessary to
assess plant growth and photosynthetic  rate in response to S02 concentrations
before a hypothesis can be formulated concerning  the increased translocation
with S02 exposure observed in this experiment.

     Photosynthetic rates are inhibited at high S02 concentrations (Bennett
and Hill, 1974; White et at., 1974; Sij and Swanson, 1974; Koziol and Jordan,
1978).  However, some data suggest a stimulation  at low S02 concentrations
(Muller et at., 1979; Katz et at., 1939; Thomas and Hill, 1937).  Low S02
concentrations apparently stimulate the Hill-reaction and benefit overall
photosynthesis whereas at higher concentration RuDP-carboxylase is inhibited
(Ziegler, 1972).  Thor (1980), in an extensive review of the S02 concentration
and photosynthetic response literature, estimated a stimulation in photosynthe-
sis may occur up to S02 concentrations  of about 20 pphm.  Measurements of the
photosynthetic rate of Agropyron smithii on our study area during the period
of this experiment showed no trend of either stimulation or inhibition (Thor,
1980).  However, in the drier previous  year 39 percent  stimulation in  the photo-
synthetic rate of Agropyron smithii was detected  on the S02 treatment.
                                      34

-------
     A significant S02 effect on net primary or Agropyron smithii productivity
could not be detected on our study area (Dodd et at., In Prep.). However mea-
suring individual leaf areas of Agropyron smith-Li, Milchunas et at. (In Prep.)
observed a significant increase in leaf areas on Zaps II Low S02 exposure
but only a trend of increased leaf area with the High treatment examined in
this study.  It was concluded that the Low treatment was optimum for stim-
ulating growth under the abiotic and nutrient conditions on our study area,
but that the High treatment had detrimental effects which were operative but
not at a level that fully negated the fertilizer effect.

     Two points are apparent from the productivity and photosynthetic responses
in conjunction with 1L|C translocation.  First, the increased 11+C translocation
with S02 exposure observed in this study is in response to stimulated growth
rates.  Second, productivity and photosynthetic rate measurements are not as
sensitive as translocation to low level S02 exposure.  Translocation was also
observed to be more sensitive to S02 than photosynthesis by Teh and Swanson
(1977) for a very high (300 pphm) S02 concentration, and by Noyes (1980)  for
concentrations of 10, 100 and 300 pphm.  They reported that translocation was
inhibited more than photosynthesis.  The inhibition of translocation with 10
pphm S02 reported by Noyes is not consistent with the increased translocation
we observed on the High treatment.  This may be attributed to several major
differences between experimental designs of the two experiments.  Noyes used
11-day-old hydroponically growing bean plants with one remaining leaf on the
plant at the time of labeling.  Translocation was monitored after the leaves
were exposed to S02 for 2 hours.  This was in contrast to our continued S02
exposure of field growing plants with the influence of intact aboveground
sinks.  Plant species, environmental conditions, S02 dose duration and concen-
tration fluctuation with possible plant adaptation, and sink demands may have
contributed to the different responses observed between the two studies.
Noyes (1980) suggested SO^ inhibited sieve-tube loading.  If this occurs, the
results from this study suggest that within a fertilizing range of low S02
dose, stimulated sink strength can override the mechanism involved in sieve-
tube loading inhibition.

     The concentration of translocated ll|C may be more sensitive to the
effects of S02 than harvest data or photosynthetic measurements both from a
technique standpoint and from a standpoint of measuring specific growth rate.
Population productivity measurements by field clip plots are subject to high
variability because of differences in species density and composition.
Subtle responses may be less than sampling variance.  Growth increments
measured with the individual plant as the unit of measure are diluted by a
factor of the variable nongrowing structural biomass.  When growth is occur<-
ring in a particular organ, the resolution of measurements of growth rate
declines as measurements proceed from the organ to the individual to the
population.  Photosynthesis is a measure of assimilation and not necessarily
utilization.  The effects of S02 manifest in biochemical pathway and functional
mechanisms after the assimilation process.  In the absence of growth, assimi-
lation may proceed at a maintenance level whereas translocation is negligible
in a sinkless system.  During growth, translocation is not entirely a function
of internal concentration gradients but is also hormonally regulated.  Divid-
ing cells produce auxins which further stimulates growth but also stimulates
phloem transport (Davies and Wareing, 1965; Patrick and Wolley, 1973; Seth

                                       35

-------
 and Wareing,  1967; Patrick, 1976).  The concentration of translocated  1IfC  is
 thus  a  sensitive  index of growth rate because of specificity  to  the particular
 organ involved  in growth.

      Differences  in  the concentration and partitioning of  14C between  Control
 and S02  exposed plants were greatest for the expanding leaf.  Although concen-
 trations of  14C in the expanding leaf were often high, this organ  received
 only  a minor  portion of the 14C pool.  Even in plants exposed to S02,  only 4
 percent  of the  total aboveground 11+C was located in the expanding  leaf.  Many
 workers  have  stressed the lack of movement of assimilate into any  but  actively
 growing  young organs or developing reproductive parts.  In this  study,  lttC
 was detected  in mature leaves but accounted for only 0.5 and  1.0 percent of
 the total aboveground ^C pool for Control and S02 treatments, respectively.
 It is not known,  however, whether the llfC entering the mature leaves was in
 sugars,  or in amino  acids synthesized in the roots and redistributed.   By  far
 the largest pool  of  exported 14C was found in the "other"  plant  parts  (Table
 4.1) where 17  and 22 percent of the aboveground lltC was partitioned in the
 Control  and S02 treatment plants, respectively.  Considering  that  1) the
 "other"  category  consisted of the stem and mature leaves excluding the  top
 three leaves, and 2) that mature leaves Imported very small quantities  of
 14C,  the majority of exported 14C was located in the stem.

     Exposure of Agropyron smithLi- on the High treatment increased iLfC  concentra-
 tions in the  belowground compartment only on the first sampling  date.   Our
 data  suggest  that this was in response to a greater rhizome sink demand.   The
 initiation of tillers is probably similar to that of developing  leaves  and
 requires  import of carbon until a self contained photosynthetic  capacity is
 attained.  Coughenour et al. (1979) labeled Agropyron smithii plant with ltfC
 on the same study area but in a previous year.  They observed stimulated root
 growth on the S02 treatment in July.  The observation of increased transloca-
 tion  to  aboveground  sinks in plants exposed to S02 concurrent with an increase
 in relative belowground 1LfC concentrations indicates a stimulation in repro-
 ductive root  and yegetatiye growth, on the High treatment.

      Data from  primary producer studies during the five years of fumigating
 this  particular grassland may at first seem contradictory.  We have observed
 S02 stimulated  translocation, photosynthesis  (Thor, 1980), and leaf areas
 (Milchunas et at., In Prep.-) concurrent with high sulfur accumulation  (Lau^
enroth et al., 1979;  Milchunas et at., 1980), increased rates of senes-
cence (Heitschmidt et al., 1978, Milchunas et al., In Prep.)  and reductions
in chlorophyll  (Lauenroth and Dodd, 1980) with no measurable  effect of S02
 on standing biomass  (Dodd et al., In Prep.)-  Other researchers  have observed
protein hydrolysis and the accumulation of free amino acids in plants exposed
 to S02 (Godzik  and Linskens, 1974; Malhotra and Sarkar, 1979; Constantinidou
and Kozlowski,  1979).  These seemingly contradictory findings can  be synthe-
 sized into a  conceptual model explaining one aspect of how S02 influences  a
plant's  life history if we differentiate between the overall  response of the
plant as  an individual or population and the organ or biochemical  components
and compare them with the known sequence of events in the  life of an unper-
turbed plant.  The hypothesis presented considers relatively  low to moderate
S02 concentrations rather than levels where immediate and acute toxic respon-
ses occur.


                                      36

-------
     The growth and senescence of plants is a complex process of nutrient
and carbon assimilation, metabolism, and distribution.  Sulfur is a required
plant nutrient and atmospheric S02 is one source of sulfur.  Thus, S02 is
both a fertilizer and a toxic gas depending on the duration and concentration
of exposure and the plant's nutrient status.  Below optimum nitrogen to sulfur
ratios were corrected in Agropyron smithii plants exposed to S02 (Milchunas
et al., 1980).  A stimulation in growth would then be expected and in-
creased leaf areas with S02 exposures confirms this (Milchunas et al., In
Prep.).  Although leaves grew at a faster rate, they also senesced at a
more rapid rate.  An increased rate of senescence has been one of the commonly
reported responses to S02 exposure  (Garsed et al., 1979; Bleasdale, 1973;
Bell and Clough, 1973; Matsushima and Harada, 1966; Heitschmidt et al., 1978;
Milchunas et al., In Prep.).  This same phenomena occurred with the applica-
tion of nitrogen fertilizer  (Milchunas et al., In Prep.).

     The question then arises as to whether the impact of S02 at low levels
is due to toxicity or a nutrient input perturbation which accelerates the
growth and senescence process.  Reductions in chlorophyll and protein hydroly-
sis occur in the natural sequence of plant senescence (Scott and Leopold,
1966).  As leaf tissue enters into senescence,  it experiences an extensive
hydrolysis of protein components (dela Fuente and Leopold,  1968;  Osborne,
1973; Abeles et al., 1967).  A wide array of amino acids accumulate as a
consequence of the protein hydrolysis, including especially glutamine (Plaisted,
1958).  With regard to the amino acid metabolism of plants  exposed to S02,
the most important changes seem to be the increase of glutamine,  NH3,  aspara-
gine, and alanine (Godzik and Linskens, 1974).   Michael (1936)  established
that the progress of leaf senescence was facilitated when soluble amide
products could be translocated out of the leaf tissues.  Further, alanine
brings about abundant ethylene production and ethylene is important in the
induction of senescence and leaf abscission (Abeles,  1967;  dela Fuente and
Leopold, 1968).  Data of Williams (1955) suggested that rapid shoot growth
could accelerate the senescence of more mature tissues by inducing the hydroly-
sis of nucleic acids.  This is supported by the observation that regions of
the plant that are rich in auxin (the young expanding parts)  (Burg and Burg,
1968) are also regions of high ethylene production (Osborne,  1973) .  Young
plant parts are not, however, susceptable to the ethylene (Abeles,  1967).
This provides a feedback mechanism for transport of nutrients from older
leaves to younger leaves.  The role of auxin as a mobilizer of  nutrients has
been well established (Addicott, 1970).

     The following is a hypothetical model of a mechanism for low-concentra-
tion S02 perturbation in the absence of visible and acute injury.  In early
spring, low concentrations of S02 supplement soil sulfur necessary for optimum
nitrogen to sulfur ratios.  Sulfur dioxide entry through leaf stomata compen-
sates for differential absorption or translocation rates of N and S.  A ferti-
lizing effect ensues which stimulates growth.  Stimulated growth in new leaves
is a strong sink which increases translocation from older leaves.  The older
leaves have now been exposed to S02 for a long period of time.   The sulfur
concentration that has built up is relatively immobil.e and does not leave  the
leaves as readily as does nitrogen  (Williams, 1955).  The build up of sulfur
causes a loss of membrane integrity releasing SF (senescence factor) which
enhances ethylene biosynthesis.  The older leaves are also susceptible to  the


                                      37

-------
ethylene produced in the young expanding leaves.  Protein hydrolysis and the
mobilization of nutrients and chlorophyll to younger plant parts ensues.  In
this manner stimulated growth and translocation, protein hydrolysis, an
increased rate of senescence, reduced chlorophyll content, with no change in
total standing biomass can all be explained.  Increased translocation rates
can be a function of the more rapid turnover and the mobilization of nutrients
as senescence proceeds .

     There appears then to be good correlation between the natural senescence
processes in plants and the responses to S02-  A relationship between sulfur
content and date of abscission in leaves of Querous rubva has been observed
(Garsed et al., 1979).  Premature leaf fall seems to be a common response of
both coniferous and deciduous trees in industrial areas, and certain trees
that are normally evergreen may be come deciduous in some polluted regions
(Scurfield, I960).

                                   CONCLUSIONS

     Exposure of Agropyron smithii Rybd.  on the High S02 treatment increased
translocation of photoassimilated lttC02 to rhizomes early in the growing
season and to developing leaves throughout the growing season.   Leaves near
the top of the plant supplied proportionately more assimilate to the developing
leaf while lower leaves partitioned a greater proportion to a S02 stimulated
rhizome sink.   Examination of productivity and photosynthesis data concurrent
with translocation responses suggested that subtle effects of low-level S02
exposure may best be monitored through -^C partitioning studies.

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Bell, J. N. B., and W. S.  Clough.  1973.   Depression of Yield in Ryegrass
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Ho, L. C.  1979.  Regulation of Assimilate Translocation between Leaves and
     Fruits in the Tomato.  Ann. Bot., 43:437-448.

Kamanina, M. S., and A. A. Anisimov.  1977.  Escape of Assimilates  From the
     Mesophyll into the Void Space of Leaves Under Different  Conditions of
     Mineral Nutrition.  Soviet Plant Physiol., 24:628-632.


                                     39

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Katz, M., G. A. Ledingham, and A. E. Harris.  1939.  Carbon Dioxide Assimila-
     tion and Respiration of Alfalfa Under Influence of Sulphur Dioxide.  In:
     Effect of Sulfur Dioxide on Vegetation.  The Associate Committee on
     Trail Smelter Smoke of the National Research Council of Canada.  206 p.

Koziol, M. J., and C. F. Jordan.  1978.  Changes in Carbohydrate Levels in
     Red Kidney Bean (JPhaseolus vulgaris L.) Exposed to Sulphur Dioxide.  J.
     Exp. Bot., 29:1037-1043.

Lauenroth, W. K., C. J. Bicak, and J. L. Dodd.  1979.  Sulfur Accumulation in
     Western Wheatgrass Exposed to Three Controlled S02 Concentrations.
     Plant and Soil, 53:131-136.

Lauenroth, W. K., and J. L. Dodd.  1980.  Chlorophyll Reduction in Western
     Wheatgrass Exposed to Sulfur Dioxide.  In;   Bioenvironmental Impact of
     a Coal-fired Power Plant,  Fifth Interim Report, Colstrip, Montana.  E.
     M. Preston and D.  0''Guinn (eds.) EPA-600/3^80-052. "U.S. Environmental
     Protection Agency, Corvallis, Oregon, pp. 197^203.

Malhotra, S. S., and S. K. Sarkar.  1979.  Effects of Sulphur Dioxide on
     Sugar and Free Amino Acid Content of Pine Seedlings.  Physiol. Plant.,
     47:223-228.

Matsushima, J., and M.  Harada.  1966.  Sulfur Dioxide Gas Injury to Fruit
     Trees.  V.  Absorption of Sulfur Dioxide by Citrus Trees and its Relation
     to Leaf Fall and Mineral Contents of Leaves.  J. Jap. Soc. Hort. Sci.,
     35:242-246.

Michael, G.  1936.  Uber die Deziehungen zwischen chlorophyll und Eiweissabbau
     im virgilbenden Laubblatt von Tropoeolwn.  Z. Botan., 29:385-425.

Milchunas,  D.  G.,  W.  K.  Lauenroth,  and J.  L.  Dodd.   In  Prep.   Effects of 862
     Exposure with Nitrogen and  Sulfur Fertilization on the  Growth of Agropyron
     smithii  Rybd.   In:   Bioenvironmental Impact  of a Coal-fired Power Plant,
     Sixth Interim Report,  Colstrip,  Montana.  E.  M.  Preston,  D.  W.  O'Guinn,  and
     R.  A.  Wilson (eds.)  Environmental Protection Agency,  Corvallis,  Oregon.

Milchunas, D. G., W. K. Lauenroth, and J. L. Dodd.  1980.  Forage Quality
     of Western Wheatgrass Exposed to Sulfur Dioxide.  J. Range Manage.

Mor, Y.,  and A. H. Halevy.   1979.  Translocation of  IL|-C-assimilates  in  Roses.
     I.  The Effect  of  the Age of  the Shoot  and  the  Location  of the  Source
     Leaf.  Physiol. Plant.,  45:177-182.

Muller, R. N., J. E. Miller,  and D.  G.  Sprugel.   1979.   Photosynthetic  Re-
     sponse of Field-grown Soybeans  to Fumigations With  Sulphur Dioxide.  J.
     Appl. Ecol., 16:567-576.

Noyes, R. D.  1980.  The Comparative Effects  of  Sulfur Dioxide on Photosyn-
     thesis and Translocation in Bean.   Physiol. Plant Pathol., 16:73-79.
                                      40

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Osborne, D. J.  1973.  Internal Factors Regulating Abscission.   In:   Shedding
     of Plant Parts, T. T. Kozlowski,  ed.   Academic Press,  New York.  pp.
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Patrick, J. W.  1976.  Hormone-directed Transport of Metabolites.  In:
     Transport and Transfer Processes  in Plants.   I. F. Wardlaw  and J. B.
     Passioura, eds.  Academic Press,  New York.   Chapter  37, p.  433-446.

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     of Acer platanoides L. Leaves.  Contribs. Boyce Thompson Inst.,  19:245-
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     77.

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     103-107.

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Thor, G. L.  1980.  Photosynthesis  in  Western Wheatgrass  Exposed to Chronic
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Thrower, S. L.  1962.  Translocation of Labelled  Assimilates in  Soybeans.
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     Aust. J. Biol. Sci., 15:629-649.

                                      41

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Wardlaw, I. F.  1968.   The Control and  Pattern  of Movement of Carbohydrates
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White, K. L., A. C.  Hill,  and J.  H. Bennett.  1974.  Synergistic Inhibition
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Ziegler, I.  1975.   The Effect of S02 Pollution on Plant Metabolism.  Residue
     Rev., 56:79-105.
                                     42

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                                  SECTION 5

         EFFECTS OF LOW-LEVEL SULFUR DIOXIDE EXPOSURE ON DECOMPOSITION
             OF WESTERN WHEATGRASS (AGROPYRON SMITHII) LITTER UNDER
                             LABORATORY CONDITIONS

                 J. W. Leetham, J. L. Dodd, and W. K. Lauenroth
                                   ABSTRACT

               A laboratory study of the effects of chronic low-
          level S02 exposure on decomposition of western wheatgrass
          (Agropyron smithi-i) was conducted.  Finely ground
          western wheatgrass litter was exposed to 8.5 pphm S02
          continuously for 5 weeks.  Samples were periodically
          measured for respiration and total decomposition.  Results
          showed a significant 9-17 percent reduction in decompo-
          sition rates under S02 exposure.   Respiration rate
          differences were not detectable with the techniques
          used.  It is speculated that lowered pH conditions
          in the litter and/or the accumulation of toxic S02
          derivatives were responsible for reduced microbial
          activity.
                                 INTRODUCTION

     Soil surface decomposition processes are responsible for the breakdown
of a majority of aboveground herbage biomass in natural grasslands.  Surface
decomposition is essential for the release of organic products into the sub-
surface nutrient cycling processes that form the basic support of the whole
ecosystem.  Any major disturbance of the decomposition processes will ulti-
mately affect all other components of the system.  A major disturbance can be a
large-scale, short-term disturbance, or a low-level, chronic disturbance which
may take considerable time to bring about major changes in the system.

     Babich and Stotzky (1974) have reviewed the literature dealing with air
pollutant interactions with microorganisms and cite numerous studies of the
toxicity of S02, especially with increasing soil acidity. Baath et al. (In Press)
and Abrahamsen et al. (1978) in Sweden and Norway respectively have shown that
artificial acidification of coniferous forest soils significantly reduced soil
microbial biomass and activity and overall decomposition of leaf litter.  Grant
et al. (1979) found reduced microbial activity in acidic forest soil when it was
exposed to 100 pphm S02.  Saunders (1973) reviewed the effects of air pollutants

                                      43

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on leaf surface microflora and cites much evidence of deleterious effects of
SC>2 on the microorganisms.  Wodzinski and Alexander (1978) provide evidence
of significant effects of SC>2 on algal photosynthetic rates.  There is consid-
erable usage of SC>2 in the food production and preservation industry to
completely inhibit various types of microbial activity.

     Dodd and Lauenroth (1979) reported up to 43 percent reductions in decompo-
sition rates in western wheatgrass leaves with chronic low-level S02 exposure
under field conditions.  It was that finding which precipitated this study for
the purpose of verifying the field data with more precise laboratory control.

                             MATERIALS AND METHODS

     The exposure system used in this study was relatively simple in design.
It consisted of a plexiglass chamber measuring 0.61 m x 0.61 m x 1.83 m  (2 ft
x 2 ft x 6 ft).  Air movement through the chamber was a single pass, push-pull
system which created a slight negative internal pressure.  Source SC>2 was
released from a temperature-stabilized bottle of liquid SC>2 directly into the
inlet air stream to create the desired S02 concentration.  An identical
chamber without SC>2 was used for the control.  The chambers were housed in a
room maintained at 24°C.  Details of the chamber construction and operation
are described by Leetham et al. (1980).

     Sulfur dioxide concentration in the treatment chamber was maintained at
8.5 pphm as measured by a flame photometric sulfur gas analyzer (Meloy Labor-
atories Inc., Model SA-160) at the exhaust fan orifice.  Because of slight
variability of S02 concentration within the chamber, other measurements were
made at various locations on the shelves where the litter samples were main-
tained.  Temporal variation in S02 concentration was less than ±1 pphm and
spatial variation did not exceed ±2 pphm for all points measured.

     Test material was predominantly western wheatgrass (Agropyron smithi-i
Rydb.) litter gathered from a native northern mixed-grass prairie site in
southeastern Montana in May, 1979.  The litter was dead material grown during
the previous (1978) growing season and had not been previously exposed to any
major air pollutants.  The litter was finely ground in a Willey mill and
thoroughly mixed to a homogenous state.  Ash content was measured by ashing
in a muffle furnace at 600°C.   Mean ash content was 12.36 percent (S.E.  =
0.17 percent) for 10 subsamples of the homogenate.   To maintain the natural
microorganism inoculate,  the litter was dried at 30°C prior to weighing out
test parcels.  Water content of the litter at 30°C was 5.15 percent (S.E. =
0.02 percent, n = 10) and was  accounted for in weight loss calculations.

     A schematic of the test sample dish is provided in Figure  5.1.  Each
sample consisted of a 2 g layer of litter over a 20 g layer of washed and
autoclaved sand in a 60 x 15 mm plastic petri dish.  The washed sand was
determined to have a mean ash-free organic content of 0.46 percent (S.E.  = 0.02
percent,  n = 10).   A small access port was made through the litter layer in
the center of the dish to allow periodic watering by trickling distilled water
through the access port into the sand.  The litter was moistened by absorption
of water from the sand rather than by surface flooding.   Since high relative
humidity was not maintained in chambers, evaporation required daily addition of


                                     44

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                                 Watering Port
                                                -60 X 15 mm
                                               Petri dish
                                                 • Litter (2 g)
                                                 •Sand  (20 g)
Figure  5.1.   Schematic of sample dish for decomposition study,
approximately 5 ml  of water per sample.  Dishes containing only sand were
maintained the same as those with litter.

     The experiment was initiated on 6 September 1979 when all litter samples
were placed in the control and S02 treatment chambers.  Samples were randomly
selected and removed for measurements on each of four sampling dates (17,  24
September and 1, 8 October).  Sample size was 10 per chamber on the first
three dates and 20 per chamber on the final date.  After removal from the
chambers the samples were watered, as during the incubation period, and
respiration rates were measured over a 4 hour test period with the alkali
absorption technique described by Coleman et at. (1978).  The samples were
then oven-dried at 60°C and weighed.  Decomposition was expressed as percent-
age loss of original ash-free dry weight.  Daily loss rates were calculated
by dividing ash-free weight-loss for a given interval by ash-free weight at
the beginning of the interval and by the duration (days) of the interval.

                             RESULTS AND DISCUSSION

     Significant respiration rate differences between treated and control
samples were not detectable.  For example, on the second sample date the
average respiration rates were 0.2531 yg C02 •  Sample"1 •  min~J (S.E.  = 0.0084)
and 0.2512 yg C02 •  Sample ^ •  min"1 (S.E. = 0.0058) for  the control and  S02
treatment respectively.  No consistent trend was observed  across time. No
respiration was detected in the dishes containing only sand.

     An obvious decrease in litter decomposition in the S02-exposed dishes
was observed on all sample dates (Figure  5.2).  A split-plot design ANOVA
was performed on the data to test for treatment and time differences.  Treat-
ment differences were significant at P = .075 and the date differences were
significant at P < .001.  Standard errors of the means for any date-treatment
ranged from 2 to 4 percent of the means.

     Decomposition rates for both the control and S02 treated samples were
greater during the first 11 days of the test (11.5 and 10.5 yg • g"1 • d"1,
respectively) than for the last 21 days of the test (4.2 and 3.5 yg • g"1  •
d"1, respectively).   This demonstrates increasing resistance of the litter
material to decay with time, a characteristic pattern in decomposition of
relatively fresh plant litter (Christie, 1979;  Howard and  Howard, 1974) which


                                      45

-------
        o
        UJ
        z-o
        < a,
        o «
        a: -i:
        CO
        CO
        o
               6 Sep
              !7Sep     24 Sep
lOct
8 Oct
 Figure  5.2.
Decomposition in control and S02 exposed western wheatgrass
litter over four sample dates.  Figures are average total
weight loss expressed as a percentage of original starting
weight (less residual water content).
 is a consequence of rapid initial decay- of labile compounds such as sugars,
 starches,  and proteins,  followed-by much slower decay of more resistant
 compounds  (cellulose,  lignin,  fats, tannins,  waxes)  (Hunt,  1977).

      Inhibition of decomposition rates by S02 was less during the first
 interval than in the last two-thirds of the test period (9 versus 17 percent
 reduction  in daily loss  rate).   This strongly suggests a cumulative effect
 of exposure to 862, since atmospheric S02 concentrations were constant, and is
 probably due to the accumulation of toxic SC>2 derivatives such as sulfate
 or sulfite or a reduction in pH of the litter-microbe system.

                                   CONCLUSIONS

      Although the significance level of the treatment differences (P = 0.075)
 exceeded the "traditional" 0.05 level of acceptance, we are concluding they
 are real since the trend is strong and consistent with time and the results
corroborate the findings  of Dodd and Lauenroth  (1979).  They reported 12-43
percent reductions in decomposition rates in response to season-long exposures
of western  wheatgrass leaves to low-level S02 under field conditions.  These
 studies present strong evidence that chronic exposure to S02 in low concentra-
 tions can  cause a significant  reduction in microbial activity in soil surface
 litter. Neither study attempted to identify the mechanisms of inhibition of
 microbial  activity. We  suspect that a reduction in pH in the litter and/or
                                      46

-------
the accumulation of toxic S02 derivatives to be the probable mode of action
of SC>2 on the microorganisms.  Other studies have found reductions in acidity
do reduce microbial activity (Abrahamsen et at, 1978; Baath et al.,  1980;
Saunders, 1973; Wodzinski and Alexander, 1978; and Grant et at.,  1979).

     The asymptotic curve of decomposition over time (Figure 5.2) was expected
because the mechanical grinding of the old, partially decomposed  litter  ex-
posed more labile material previously unavailable to the microorganisms  and
they quickly acted upon it.  Had the study been carried out over  a longer
period of time, the curve undoubtedly would have flattened out even more,  but
we suspect treatment differences would have been magnified.

     Respiration rate differences were not detected probably because of  the
technique used.  We suspect the respiration rates were different  since respi-
ration is a good index to microbial activity and we are concluding that  the
microbial activity was reduced by S02.  More refined techniques of respiration
measurement would be needed to accurately measure the small differences  that
probably occurred in our experimental design.

                                  REFERENCES

Abrahamsen, G., J. Hovland, and S. Hagvar.  1978.  Effects of Artificial Acid
     Rain and Liming on Soil Organisms and the Decomposition of Organic
     Matter.  SNSF-contribution FA 28/78.  23 pp.

Baath, E., B. Berg, U. Lohm, B. Lundgren, H. Lundkvist, T. Rosswall, B.
     Soderstrom, and A. Wiren.  1980.  Effects of Experimental Acidification
     and Liming on Soil Organisms and Decomposition in a Scots Pine  Forest.
     Pedobiologia (in press).

Babich, H., and G. Stotzky.  1974.  Air Pollution and Microbial Ecology.
     Grit. Rev. Environ. Control, 4:353-421.

Christie, E. K.  1979.  Ecosystem Processes in Semi-arid Grasslands.  II.
     Litter Production, Decomposition, and Nutrient Dynamics.  Aust. J.
     Agric. Res., 30:29-42.

Coleman, D. C., R. V. Anderson, C. V. Cole, E. T. Elliott, L. Woods, and M.
     K. Campion.  1978.  Trophic Interactions in Soils as they Affect Energy
     and Nutrient Dynamics.  IV-  Flows of Metabolic and Biomass  Carbon.
     Microbial Ecology, 4:373-380.

Dodd, J. L., and W.  K. Lauenroth.   1980.     Effects of Low-level S02 Fumi-
     gation on Decomposition of Western Wheatgrass Litter in a Mixed-Grass
     Prairie.   In:  Bioenvironmental Impact of a Coal-fired Power  Plant.
     Fifth Interim Report,  Colstrip,  Montana.  E. M.  Preston and  D.  W.
     O'Guinn (eds.)   EPA-600/3-80-052.  U. S. Environmental Protection
     Agency, Corvallis, Oregon, pp. 212-215. (In Press).

Grant, I. F.,  K. Bancroft,  and M. Alexander.  1979.  S02 and N02  Effects on
     Microbial Activity in an Acid Forest Soil.  Microbial Ecology,  5:85-89.
                                      47

-------
Howard, P. J. A. and D.  M.  Howard.   1974.   Microbial  Decomposition  of  Tree
     and Shrub Leaf Litter.  I.   Weight Loss  and  Chemical  Composition  of
     Decomposing Litter.  Oikos,  25:341-352.

Hunt, H. W.  1977-   A Simulation Model for  Decomposition in  Grasslands.
     Ecology, 58:469-484.

Leetham, J. W.,  W.  Ferguson,  J.  L.  Dodd, and  W. K. Lauenroth.   1980.   Design
     and Construction of a Simple,  Continuous Flow Sulfur  Dioxide Exposure
     Chamber (In Press).

Saunders, P. J.  W.   1973.   Effects  of  Atmospheric Pollution  on  Leaf Surface
     Microflora. Pestic.  Sci.,  4:589-595.

Wodzinski, R. S., and M. Alexander.  1978.  Effects of Sulfur Dioxide  on
     Algae.  J.  Environ. Qual.,  7(3):358-360.
                                     48

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                                   SECTION  6

         IMPACT OF  S02 EXPOSURE  ON THE  RESPONSE OF WESTERN WHEATGRASS
                       (AGROPYRON SMITHII)  TO DEFOLIATION

                  W. K. Lauenroth,  J. K. Detling and J. L. Dodd
                                    ABSTRACT

               Agropyron  smithii populations exposed to three
          controlled  S02  concentrations were defoliated either
          once or  twice during  the growing season at either a
          light  or heavy  rate.

               Interactions between S02 exposure and defoliation
          occurred with respect to biomass, number of tillers
          and sulfur  uptake.
                                  INTRODUCTION

     During  the  first four years of a field experiment regarding the response
of a North American grassland  to controlled low concentrations of sulfur
dioxide  (Heitschmidt et al. , 1978) we have accumulated evidence that exposures
during the growing season had  subtle but potentially important effects upon
the system (Lauenroth and Heasley, 1980).  For example, S02 exposure reduced
chlorophyll  concentrations and increased sulfur contents in several important
species  (Lauenroth et al., 1979; Lauenroth and Dodd, In Prep.)., decreased the
functional lives of leaves of  the dominant species, western wheatgrass
(AgvopyTon smithii Rydb.) (Heitschmidt et at., 1978) and decreased the amount
of carbon stored in the rhizomes of western wheatgrass (Lauenroth and Heasley,
1980).

     Growth  initiation of western wheatgrass in the spring and after defolia-
tion is  dependent upon carbohydrates stored in rhizomes and roots (Bokhari,
1977).   Before the S02 treatments were begun the area had been grazed by
cattle.  Following exclusion of cattle rhizome biomass increased significantly
on the Control.  In contrast,  rhizome biomass failed to recover on the 8.0
pphm S02 treatment, suggesting that S02 exposure was having an effect similar
to grazing.  Populations under stress are often more susceptible to damage
caused by additional perturbations (Weinstein and McCune, 1979) .  Because of
the importance of these grasslands to the regional livestock economy and the
high probability that coal combustion for electric power production will


                                      49

-------
increase in this area we designed a field experiment to examine the potential
interactions between defoliation and S02 exposure on the native vegetation.

                             MATERIALS  AND METHODS

     This experiment utilized a split-split-plot design with S02 as the main
treatments and defoliation intensity as split-plots and defoliation frequency
as the split-split-plots.  The three defoliation intensities were (none,
light, and heavy) and the two frequencies were (once or twice per season).
Each of the S02 treatment plots encompassed 0.52 ha and within each were
located five replications of each defoliation treatment.  Each defoliation
treatment was applied to one half square meter.

     The heavy defoliation treatment consisted of hand clipping all of the
live aboveground biomass and the light treatment removed 50 percent.  The
single defoliation occurred on 20 May when aboveground live biomass of
western wheatgrass is typically near 30 percent of the growing season maximum
 (Dodd et at., 1979.  The second defoliation treatment occurred on 20 June,
near the time of expected peak live biomass.

     All experimental plots were harvested on 15 August.  Aboveground biomass
was clipped at the soil surface and separated by species.  Each sample was
then oven-dried at 60°C for at least 72 hours and weighed.  At the time of
harvesting the number of tillers of western wheatgrass were counted in each
plot.  Subsamples of western wheatgrass were analyzed for total sulfur using
a Leco Induction Furnace (Laboratory Equipment Co., St. Joseph, MI.).

     The data were subjected to a split-split-plot analysis of variance of
S02 treatments and defoliation intensity and frequency (Table 6.1).    Differ-
ences between individual means were tested using Tukey's Q procedure (Snedecor
and Cochran, 1967).

                                     RESULTS

     On 15 August, total aboveground biomass (all species) was significantly
(P < 0.01)  altered by the interaction of clipping intensity and clipping fre-
quency.  The main effects and interactions with S0£ were nonsignificant
Total aboveground biomass was unchanged as a result of the single clipping
regardless of the intensity (Figure 6.1).   Reapplication of the clipping
treatments resulted in significant decreases in total biomass at both clipping
intensities.

     Biomass of western wheatgrass responded significantly to the interactions
of S02 x clipping frequency (P = 0.05)  and clipping intensity x clipping fre-
quency (P = 0.001).  The latter indicated that standing crop of western
wheatgrass was unchanged by the single clipping but significantly decreased
by reclipping at both the moderate (50 percent decrease) and heavy  (90 percent
decrease) intensities (Figure 6.2a).  The S02 x clipping frequency interaction
indicated that western wheatgrass responded differently to S02 as a result of
being clipped once or twice (Figure 6.2b).   The single defoliation resulted in
significant decreases in western wheatgrass biomass at the Medium and High
S02 concentrations compared to the Control.   As a result of reapplying the

                                      50

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          TABLE  6.1.   RESULTS OF ANALYSIS OF VARIANCE
          Source of variation
                                             df
          S02


          Rep (S02)


          Defoliation Intensity (DI)


          DI x S02


          Error B


          Defoliation Frequency (DF)


          DF x S02


          DF x DI


          DF x S02 x DI


          Error C


          Total
                                              3


                                             16


                                              2



                                              6


                                             32


                                              1



                                              3


                                              2


                                              6


                                             48


                                            119
                          60 r
Figure  6.1.
                         40
                      E

                      o>

                      V)
                      CO
                      <
                      s
                      o
                      m   20
                Undipped    Light      Heavy


                     CLIPPING  TREATMENT


Response of total aboveground biomass to three defoliation

intensities and two defoliation frequencies (i     I  = once,

 Y//////\ = twice) .


                       51

-------
         20
     2  treat-
ments which were apparent after  the single  clipping were no  longer present.
This was largely the result of the large impact  of reapplying  the  heavy
clipping treatment (Figure  6.2a).

     Analysis of variance of western wheatgrass  tiller  density identified
significant differences as a result of  the  S02 x clipping  frenquency  (P =
0.08), and clipping intensity x  clipping frequency  (P = 0.001)  interactions.
The interaction of clipping intensity and a single defoliation resulted in a
nonsignificant increase in tillers  as a result of light clipping and  a
significant increase as a result of the heavy clipping  (Figure  6.3a).
Reapplication of the light clipping treatment resulted  in  no change in tiller
density, but there was a large (65  percent)  significant decrease following re^
application of the heaviest clipping treatment.   The S02 x clipping frequency
interaction, while not fitting traditional  limits of significance  (P  < 0.05),
does provide important information.  These  results  indicated (Figure   6.3b)
that western wheatgrass tiller density  was  decreased by all  S02 treatments
regardless of clipping intensity at the time of  the initial  clipping.  Reappli-
cation of the clipping treatment resulted in additional decreases  in  tiller
density.

     Sulfur concentration in western wheatgrass  was significantly  altered by
the three-way interaction of S02,  clipping  intensity and clipping  frequency
(P = 0.02).  Sulfur content was  closely related  to  S02  concentration  regardless
of clipping intensity or frequency (Figure   6.4). A single  clipping  treatment

                                     52

-------
      200
                     a    300
                                        200
  a>
       100
  UJ
                                         100
            Undipped  Light    Heavy
                                                      8
Figure  6.3.
 CLIPPING  TREATMENT        S02  CONCENTRATION (pphm)
 Response of western wheatgrass  tiller density (a) to three
 defoliation intensities and two defoliation frequencies
 (f      I = once, ZZZZZZZa = twice); (b) to S02  concentrations
 at two defoliation frequencies  (	 = once,	= twice).
       4000r
    o>

    C7>
    oc
    ID
       2000
           0
             0
                                     a
                 68     0246

                  S02 CONCENTRATION  (pphm)
8
Figure  6.4.
Response of  sulfur concentration in western wheatgrass to SC>2
concentration, defoliation intensity and one  (a) or two (b)
defoliations  (	= undipped, —	= light, 	 =
heavy).
                                   53

-------
resulted  in similar rates of increase in sulfur content with increases in  S02
concentration regardless of the intensity of clipping  (Figure   6.4a).  The
light clipping  treatment did not significantly alter sulfur content, compared
to undipped plants but the heavy clipping treatment significantly increased
sulfur content  of western wheatgrass at all but the lowest S02  concentrations.
Reclipping of western wheatgrass plants altered the rate of sulfur accumula-
tion compared to the undipped plants (Figure  6.4b).  Sulfur content of
plants subjected to the heaviest clipping treatment was significantly greater
than undipped plants at the Control, Low/,  and Medium S02 treatments but not
at the Highest S02 treatment.  In contrast,  the sulfur content of plants
subjected to the light clipping treatment were not significantly different
from the undipped plants at the Control, Low and Medium S02 treatments but
were signficantly different at the Highest S02 concentration.

     Standing crop of sulfur in western wheatgrass (Table  6.2)  indicated
that sulfur uptake was a function of S02 concentration for undipped and
clipped plants regardless of the degree of  defoliation.  The amount of sulfur
taken up was largely unaffected by a single  clipping and substantially altered
by reclipping.  Reapplying the light clipping treatment resulted in a decrease
of approximately one-half in standing crop  sulfur at each S02 concentration.
At the heaviest clipping intensity reclipping decreased the standing crop of
sulfur on the Control and Low S02  treatments by a factor of 8 and on the
Medium and High S02 treatments by  a factor of 6.

     The rate of sulfur uptake (standing crop divided by accumulation period)
could not be calculated for the light defoliation treatment because of the
complications posed by the stubble.   Uptake  of sulfur was doubled by a single
heavy defoliation at the Control and Low treatment concentrations and increased
TABLE  6.2.    STANDING CROP (mg) AND SULFUR UPTAKE RATE (mg day"1) FOR
               WESTERN WHEATGRASS SUBJECTED TO CLIPPING AND S02 TREATMENTS
S02
                                        Clipping Treatment
Treatment
Control
Low
Medium
High
Undipped*
17C.125)
21(.154)
24(.176)
44(.324)
Once
18
26
23
48
Light
Twice
9
13
11
22
Once
19(.218)
25(.287)
25(.287)
36(.414)
Heavy
Twice
2(.036)
3 (.054)
4C.072)
6(.107)

   All undipped results combined.
                                      54

-------
by 50 percent at the Medium and High S02 concentrations.  Reapplying the
heavy defoliation sharply decreased rate of uptake to one-third of that cal-
culated for undipped plants.

                                   DISCUSSION

     While we observed  important  interactions between S02 exposure and defolia-
tion treatments, the majority of  our results indicated  that the intensity and
frequency of defoliation were most influencial in determining the growth and
tillering responses we  observed.  Interactions between  S02 and either biomass
(Figure  6.2b) or tiller density  (Figure  6.3b) of western wheatgrass represent
potentially important indications of the state of the system after exposure
to S02.  Whether these  results would be compensated for or compounded by
subsequent seasons of S02 exposure and defoliation must be determined before
the long-term consequences of these interactions can be determined.  In this
regard, it is interesting to note that a single clipping applied early in the
growing season had no significant effect on final total biomass of all species
(Figure  6.1) or that of western  wheatgrass (Figure  6.2a).  Although direct
estimates of aboveground net primary production (ANPP) were not made, these
results suggest that ANPP was stimulated by a single defoliation early in the
season, regardless of intensity.  Since estimates of amount of shoot material
removed at each clipping were not made, it is not possible to infer confidently
the effects of two defoliations on ANPP.  In spite of many reports of declines
in ANPP following grazing (Jameson, 1963), reports of compensatory growth, or
even increases in plant yield following light to moderate levels of defolia-
tion,  are common (McNaughton, 1979; Harris, 1974).  Such compensatory growth
following grazing in grasslands may result from a number of indirect effects
on microclimate, such as increasing light penetration to lower leaves in the
canopy or reducing evapotranspiration and prolonging the period of favorable
soil moisture during drought (McNaughton, 1979) .  In addition, individual
plants frequently respond to defoliation by increasing photosynthetic rates
in remaining undamaged  leaves or  newly developing leaves (Detling et at.,
1979; Painter and Detling, 1980), and increasing the proportion of current
photosynthate allocated to synthesis of new leaves (Detling et al., 1980
Ryle and Powell, 1975).  Under laboratory conditions, western wheatgrass did
not appear to change its photosynthate allocation patterns in response to
differential tiller defoliation,  however,  (Painter and  Detling, 1980).

     The tillering response of grasses to defoliation is probably affected by
interactions among internal factors, such as stage of development and hormone
concentration, and external environmental factors, such as light, temperature,
or photoperiod (Goodin, 1972; Laude, 1972) .  Thus, when defoliation results
in removal of only leaves, tiller production is often depressed since available
carbohydrates are apparently utilized for production of new tillers only if
the demand for the growth of current leaves has been met already (Youngner,
1972).  Tillering may be enhanced by defoliation, however, if apical meristems
are removed, and hence  apical dominance is destroyed (Youngner, 1972).  Under
laboratory conditions,  western wheatgrass produced about the same number of
tillers regardless of level of defoliation up to removal of 75 percent of the
tillers (Painter and Detling, 1980), a finding which is generally consistent
with the relatively small change  in tiller density under all clipping treat-
ments except in those plots receiving two complete defoliations (Figure 6.4).

                                      55

-------
     Defoliation intensity and frequency produced a clear interaction with
S02 exposure in influencing sulfur uptake (Figure  6.4).  We would expect
this to be of short-term importance only if increased sulfur content of the
forage influenced forage palatability or digestability.  If either are affect-
ed, exposure to S02 will be most important in determining this response.  The
small increment in sulfur concentration as a result of clipping will be of
lesser importance.  McNary  (1980)  found that  grasshoppers  discriminate
against western wheatgrass plants grown on the S02 treatments.  The explanation
for this may reside in their differing sulfur contents.  Rumsey (1978)
reported reduced intake by cattle of a feed high in sulfur.

     At the beginning of the experiment we hypothesized that the lack of
recovery of rhizome biomass, after protection from grazing, was an indication
that S02 exposure was creating a condition of stress within the western
wheatgrass population (Esch e~b at., 1975; Lauenroth et at., 1978).  Addition-
ally we believed that by subjecting the population to an additional stress or
(defoliation) we would observe a large negative response which would be pro-
portional to the amount of stress resulting from S02 exposure.  To a large
degree the response we observed did not support these hypotheses.   Perhaps a
single season of defoliation was not sufficient to produce the expected re-
sponse.  It is also possible that rhizome biomass is not as sensitive an
indicator as we believed.  As a result of a single season investigation of
the interactions between S02 exposure and defoliation it appears that increased
sulfur loading of system components may be the most significant response
threatening long-term system stability.

                                   CONCLUSIONS

     Subjecting an Agropyron smithii population, which was hypothesized to be
in a stressed condition as a result of S02 exposure, to the additional perturba-
tion of defoliation produced only a few responses which would not  have been
expected from defoliation alone.

     Increased sulfur loading of system components may be the most important
response in terms of long-term system integrity.

                                 REFERENCES

Bokhari, U. G.  1977.  Regrowth of Western Wheatgrass Utilizing l'*C Labeled
     Assimilates Stored in Belowground Parts.   Plant and Soil, 48:115-127.

Detling, J. K., M. I. Dyer, and D. T. Winn.  1979.  Net Photosynthesis, Root
     Respiration, and Regrowth of Boutetoua graaitis Following Simulated
     Grazing.  Oecologia, 41:127-134.

Detling, J. K., M.  T. Dyer, C.  Procter-Gregg,  and M. T. Winn.  1980.   Plant-
     herbivore Interactions:  Examination of Potential Effects of  Bison Saliva
     on Regrowth of Boutetoua gracitis (H.B.K.) Lag.  Oecologia.
                                      56

-------
Dodd, J. L., W. K. Lauenroth, G. L. Thor, and M. B. Coughenour.  1978.  Effects
     of Chronic Low Level S02 Exposure on Producers and Litter Dynamics.  In:
     E. M. Preston and T. L. Gullett (eds.) The Bioenvironmental Impact of a
     Coal-fired Power Plant,  Fourth Interim Report, Colstrip, Montana. EPA-
     600/3-79-044. U. S. Environmental Protection Agency, Corvallis, Oregon.
     pp. 384-393.

Esch, G. W., J. W. Gibbons and J. E. Bourque.  1975.  An Analysis of the Rela-
     tionship Between Stress and Parasitism.  Amer. Midi. Nat. 93:339-353.

Goodin, J. K.  1972.  Chemical Regulation of Growth in Leaves and Tillers.
     pp. 135-145.  In:  V. B. Youngner and C. M. McKell (eds.) The Biology and
     Utilization of Grasses, pp. 292-303.  New York and London, Academic Press.

Harris, P.  1974.  A Possible Explanation of Plant Yield Increases Following
     Insect Damage.  Agro-ecosystems, 1:219-225.

Heitschmidt, R. K., W. K. Lauenroth, and J. L. Dodd.  1978.  Effects of Con-
     trolled Levels of Sulfur Dioxide on Western Wheatgrass on a Southeastern
     Montana Grassland.  J. Appl. Ecol., 14:859-868.

Jameson, D. A.   1963.  Responses of Individual Plants to Harvesting.  Bot. Rev.,
     29:532-594.

Laude, H. M.  1972.  External Factors Affecting Tiller Development,  pp. 164-
     154.  In:  V. B. Youngner and C. M. McKell, (eds.) The Biology and
     Utilization of Grasses, pp. 292-303.  New York and London,  Academic Press.

Lauenroth, W. K., J. L. Dodd and P. L. Sims.  1978.  The Effects of Water and
     Nitrogen Induced Stresses on Plant Community Structure in a Semi-arid
     Grassland.  Oecologia, 36:211-222.

Lauenroth, W.  K., and J. E. Heasley.  1980.   Impact  of  Sulfur Deposition on
     Grassland Ecosystem. In:   D. S.  Shriner (ed.)  Atmospheric Sulfur Deposi-
     tion:  Environmental Impact and Health Effects.  Ann Arbor  Science Pub-
     lishers,  Ann Arbor, Michigan.

Lauenroth, W. K., C. J. Bicak, and J. L. Dodd.  1979.  Sulfur Accumulation in
     Western Wheatgrass Exposed  to Three Controlled S02 Concentrations.  Plant
     and Soil, 53:131-136.

Lauenroth,  W.  K., and J.  L. Dodd. In Prep.  Chlorophyll Reduction in Western
     Wheatgrass Exposed to Sulfur Dioxide.

McNary T.  J.,  J.  W.  Leetham,  W.  K.  Lauenroth, and J. L. Dodd.  1980.  Re-
     sponse of Rangeland Grasshopper Populations to Controlled Levels of S02.
     In: E.  M.  Preston and D.  W.  O'Guinn (eds.)   The Bioenvironmental Impact
     of a Coal-fired Power Plant, Fifth Interim  Report, Colstrip, Montana.
     EPA-600/3-80-052.  U.S. Environmental Protection Agency,  Corvallis,  Oregon.
     pp. 272-278.
                                      57

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McNaughton, S. J.  1979.  Grazing as an Optimization Process:  Grass-ungulate
     Relationships in the Serengeti.  Am. Nat., 113:691-703.

Painter, E. L..and J. K. Detling.  1980.  Effects of Defoliation on Net
     Photosynthesis and Regrowth of Western Wheatgrass.  J. Range Manag.

Rumsey, T. S.  1978.   Effects of Dietary Sulfur Addition anrl Synovex-S in Ear
     Implants on Feedlot Steers Fed an All-concentrate Finishing Diet.  J. An.
     Sci., 46(2):463-477.

Ryle, G. J. H. and C. E. Powell.  1975.  Defoliation and Regrowth in the
     Graminaceous Plant:  The Role of Current Assimilate.  Ann. Bot., 39:297-
     310.

Snedecor, G.  W., and W. G.  Cochran.  1967.  Statistical Methods.  Iowa State
     Univ. Press, Ames.

Weinstein, L. H., and D. C. McCune.  1979.  Air Pollution  Stress.  In:
     Crop Plants.  H. Mussell and R. Staples  (eds.) John Wiley and Sons,
     Inc.

Youngner, V.  B.  1972.  Physiology of Defoliation and Regrowth.  In:  The
     Biology and Utilization of Grasses.  V. B. Youngner and C. M. McKell
     (eds.)  New York and London, Academic Press.  pp. 292-303.
                                      58

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                                  SECTION 7

            RESPONSE OF BOUTELOUA GEACILIS TO CONTROLLED S02 EXPOSURE

             W.K.  Lauenroth,  J.K.  Detling,  C.J.  Bleak,  and  J.L.  Dodd


                                    ABSTRACT

               Bouteloua graoilis, an Important warm season grass
          native to the Great Plains of North America, was grown
          hydroponically and exposed under field conditions to con-
          trolled concentrations of S02 .  After 31 days of exposure
          individual plants were harvested and biomass accumulation
          and sulfur content were measured.

               We found no impact of S02 on live shoot weights, root
          weights, shootrroot ratios or number of tillers.   Signifi-
          cant differences were found for crown weights and the
          ratios of live to dead shoot weights.
                                  INTRODUCTION

     Early investigations regarding the effects of sulfur dioxide on plant
growth focused largely upon short-term (hours) high concentration impacts
(Thomas, 1961).  Recently, a number of workers have investigated physio-
logical impacts of low concentrations for long time periods (weeks to months)
(Ashenden and Mansfield, 1977; Tingey and Reinert, 1975; Crittenden and Read,
1979; Bell et at., 1979).  Sulfur dioxide impacts on grasslands are receiving
considerable attention in Great Britain largely because of the importance of
a single S02 sensitive species, Lol'Lim pevenne L.  Although there is not
general agreement about its specific responses or the threshold concentra-
tions which elicit those responses, there is general agreement that perennial
ryegrass responds to low concentrations of S02 (Cowling et al. , 1973; Bell
and Clough, 1973; Bell et at., 1979).

     North American grasslands are considerably more diverse than those in
Great Britain (Lauenroth, 1979) and have only recently received attention
with regard to potential impacts of S02 (Heitschmidt et al. , 1978; Ferenbaugh,
1978; Coughenour et al., 1979).  Coincidentally, all of this work has been
focused upon the responses of C3 grasses to sulfur dioxide.  Because stomatal
behavior is very important in determining responses of plants to S02 exposure
(Winner  and  Mooney,  1980) the differences in stomatal control of photo-
synthesis observed between C3 and C^ plants (Ko"rner et al., 1979) may result

                                      59

-------
in quite different responses to S02.  Our objectives here are to report an
experiment which was designed to utilize a unique field exposure facility
(Heitschmidt et al., 1978) to evaluate the impact of S02 on the growth of a
native C^ grass Bouteloua graci-lls H.B.K. Lag.  Bouteloua gTaoi-lls is an
important dominant over much of the Central and Southern Great Plains of
North America and is an important co-dominant on many sites in the Northern
Great Plains (Lauenroth et al., 1980).

                            MATERIALS AND METHODS

     Bouteloua gTacills plants were grown from seeds in flats containing ver-
miculite until they were 30-days old.  At that time they were sorted for a
uniform size and placed in 12-liter hydroponic containers with 0.143-strength
Hoaglands solution (Detling et al., 1979).  Sponge-stoppers held the 12
plants upright in each container.   The experiment was begun on 13 July when
one container was placed in each of the S02 treatment plots and progressed
until 15 August.  Containers with hydroponically grown Bouteloua graa-il-is
plants were randomly located within each S02 treatment and buried so that
plants had a normal position within the grassland canopy.  Nutrient solutions
were replenished daily and the entire contents of the containers were changed
each week.  It was necessary to cover the containers with a wire mesh to
prevent grazing by grasshoppers.

     At the end of the experiment tillers were counted and plants were oven-
dried at 60°C until they reached a constant weight.  Each plant was then sep-
arated into four components, 1) live shoots, 2) dead shoots, 3) crowns, and
4) roots.  Dry weights were measured for each component.  Sub-samples of live
aboveground and live belowground material were analyzed for total sulfur con-
tent using a Leco Induction Furnace (Laboratory Equipment Co.).

     The results were statistically analyzed using analysis of variance.
Tukey's Q values were used to calculate least significant ranges (Sokal and
Rohlf, 1969).

                             RESULTS AND DISCUSSSION

     After 31 days exposure of Bouteloua graoilis to controlled levels of
sulfur dioxide in the field, we found no statistically significant (P = 0.05)
changes in live shoot weights, root weights, shoot:root ratios or number of
tillers (Table  7.1).  Significant differences were found for crown weights
(Table  7- 1) (P < 0.03) and the ratio of live to dead shoot weights (Figure
 7.1)  (P < 0.001).

     Bouteloua graailis is a hemicryptophyte with the crowns representing the
origin of the perennating buds as well as an important storage location for
labile carbohydrates.  The potential long-term implications of reduced crown
biomass include a reduction in the number of active stem meristems and a de-
creased supply of carbohydrates for growth initiation and regrowth after
defoliation.   Lauenroth and Heasley (1979) reported a similar effect in the
C3 cryptophyte Agropyron smlthi-i Rybd.  Exposure to S02 reduced the amount of
carbon stored in rhizomes.  Tingey and Reinert (1975)  found a much larger im-
pact of S02 exposure on Medloago sativa L. roots than shoots.  Although a


                                      60

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TABLE  7.1.
    DRY WEIGHTS OF LIVE SHOOTS,  ROOTS AND  CROWNS,  SHOOT:ROOT
    RATIOS AND NUMBER OF TILLERS PER PLANT FOR BOUTELOUA
    GRACILIS EXPOSED TO FOUR CONTROLLED  LEVELS OF  S02

S02 Cone.
(pphm)
<0.85
2.1
4.4
6.5
S.E.UI df)

Shoot
(mg)
588
657
605
514
75
Plant Part
Root
(mg)
284
247
244
252
30

Crown
(mg)
290
293
223
193
29

Shoot: Root
1:99
2:66
2:45
2:79
0:44
Number of
tillers
40
34
31
35
3

               40r
           m   30
           5
           o
           o
LU
Q
^
UJ
>
               20
               10
                0
                                                       _L
                          2468
                             S02 CONCENTRATION (pphm)
Figure  7.1.
    Ratio of live to dead shoot weights of  Bouteloua  graailis
    exposed to S02 treatments.
                                      61

-------
definitive translocation study showing reduced carbon transport to perennating
and/or belowground organs has not been reported, circumstantial evidence sup-
ports this hypothesis.

     At the lowest concentration of S02 the live to dead shoot biomass ratio
was increased significantly (P = 0.05) while at the two highest concentrations
a significant reduction in the ratio was observed.  Heitschmidt e~b at.
(1978) reported an increase in the number of live leaves per plant of Agropyron
smithi-L, as a result of exposure to S02 and a decrease in the proportion of
dead leaves in July for the 2.1 pphm treatment.  In addition they found
increased proportions of dead leaves at the 4.4 and 6.5 pphm treatments in
June.  Ferenbaugh (1978) found that the €3 grass, Ovyzopsis hymenoi-d.es Roem.
& Schult. was unaffected by S02 concentrations below 13.5 pphm except for a
decrease in total chlorophyll content at 6.2 pphm.  Cowling and Koziol (1978)
exposed another C3 grass, Lo'Lium pevenne, to three controlled S02 concentra-
tions, beginning on the 41st day after germination and continuing for 49
days.  They found no significant effects on dry weight of shoots, sp_ecific
leaf area, net photosynthesis, dark respiration or transpiration coefficient.
Following harvesting and 21 days of regrowth they found only a small significant
decrease in the specific leaf area at the 15.4 pphm treatment.  These findings
contrasted those of an early study with the same species and the same concen-
trations of S02 in which the yield of shoots was reduced (Lockyer et at. ,
1976).

     Sulfur concentration in shoots of Bouteloua gicaoit-Ls not exposed to the
S02 treatments was 1800 yg • g"1 (Figure 7.2).  Exposure to the high concentra-
tion treatment significantly (P < 0.01) increased this to 2200 yg • g
                                                                     -1
            4000
            3500
            3000
         LJ
         8  2500
         ID
         C/5
            2000
            1500
                   o	o Root  sulfur
                   •	• Shoot  sulfur
                         _- o.
                0246
                    S02  CONCENTRATION (pphm)
                                                       8
Figure  7.2.   Shoot and root sulfur content of Bouteloua gvaoilis exposed to
               three controlled SC-2 treatments.
                                      62

-------
Lauenroth et al.  (1979) reported that average shoot sulfur contents of
Agvopyron smithii, indigenous  to the experimental site, ranged from 800 to
1100 yg • g"1.  Exposure  to the High. S02 treatment increased these values at
the rate of 385-650 yg  •  g"1 month"1.  End of the growing season sulfur
concentrations were in  the range of 3000-5000 yg • g"1.  Root sulfur concentra-
tions for blue grama were higher than shoot concentrations by approximately
60 percent (Figure  7.2).  Bicak et al. (In Prep.) reported root and shoot
sulfur concentrations for Agropyron smithii grown in a similar hydroponic
system and exposed to S02 concentrations in the control and high treatments.
Shoot sulfur content was  approximately 20 percent greater than root sulfur
content after a 6-day exposure period in June.  Shoot and root sulfur contents
were equal after  a 6-day  exposure in July_.  Cowling and Lockyer (1978) reported
no effect of S02  exposure on the root sulfur content of Lolium perenne and
shoot sulfur contents were 2 to 3 times larger than roots.

                                 CONCLUSIONS

     Our hypothesis that  differences in physiological behavior between C^ and
C3 plants would result  in different responses to S02 exposure was not sub-
stantiated by results from the experiment.  Responses of C^ grass Bouteloua
gi>aci1is were largely similar  to those previously reported for C% grasses.

                                 REFERENCES

Ashenden, T. W.,  and T. A. Mansfield.  1977.  Influence of Wind Speed on the
     Sensitivity  of Ryegrass to S02.  J. of Exp. Bot., 28:729-735.

Bell, J. N. B., and W.  S. Clough.   1973.  Depression of Yield in Ryegrass Ex-
     posed to Sulfur Dioxide.  Nature, (London) 241:47-49.

Bell, J. N. B., A. J. Rutter,  and J. Relton.  1979.  Studies on the Effects
     of Low Levels of Sulfur Dioxide on the Growth of Lolium perenne L.  New
     Phytol., 83:627-643.

Bicak, C. J., W. K. Lauenroth,  J. L. Dodd.  In Prep.   Sulfur Distribution and
     Allocation in Western Wheatgrass Exposed to S02 Under Variable Nutrient
     Sulfur Regimes.  In:  Bioenvironmental Impact of a Coal-fired Power Plant.
     Sixth Interim Report, Colstrip, Montana.  E. M.  Preston, D.  W. O'Guinn,
     and R. A. Wilson (eds.)   U.S. Environmental Protection Agency, Corvallis
     Oregon.

Coughenour, M. B., J. L.  Dodd,  D. C. Coleman, and W.  K. Lauenroth.  1979.
     Partitioning of Carbon and S02 in a Native Grassland.  Oecologia, 42:
     229-240.

Cowling, D. W., L. H. P.  Jones, and D. R. Lockyer.  1973.  Increased Yield
     Through Correction of Sulfur Deficiency in Ryegrass Exposed to Sulfur
     Dioxide.  Nature,  (London) 243:479-480.
                                      63

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Cowling, D. W., and M.  J.  Koziol.   1978.   Growth of  Ryegrass  (Lolium perenne
     L.) Exposed to S02.  I.  Effects on Photosynthesis  and Respiration.   J.
     of Exp. Bot., 29:1029-1036.

Cowling, D. W., and D.  R.  Lockyer.  1978.  The Effect of S02  on Lol-ium perenne
     L. Grown at Different Levels  of Sulfur and Nitrogen Nutrition.  J. Exp.
     Bot., 29:257-265.

Crittenden, P. D., and D.  J. Read.  1979.  The Effects of Air Pollution on
     Plant Growth with Special Reference to Sulfur Dioxide.   III.   Growth
     Studies with Loliwn multiflorim lam. and Daotylis glomevata L.  New
     Phytol., 83:645-651.

Detling, J. K., M. I.  Dyer, and D. T. Winn.  1979.  Net  Photosynthesis, Root
     Respiration, and Regrowth of  Bouteloua grac-fl-ls Following Simulated
     Grazing.  Oecologia,  41:127-134.

Ferenbaugh, R. W.  1978.  Effects  of Prolonged Exposure  of Ovyzops-is hymeno-ides
     to S02.  Water, Air,  and Soil Pollut., 10:27-31.

Heitschmidt, R. K., W.  K.  Lauenroth, and J. L. Dodd.   1978.   Effects of Con-
     trolled Levels of Sulfur Dioxide on Western Wheatgrass in a Southeastern
     Montana Grassland. J. of Appl. Ecol., 14:859-868.

K3rner,  c •> J- A. Scheel  and H. Bauer.   1979.  Maximum  Leaf  Diffusive Conduc-
     tance in Air Plants.   Photosynthetica, 13:45-82.

Lauenroth, W. K.  1979. Grassland Primary Production:  North American Grass-
     lands in Perspective.  In:  N. R. French (ed.)  Perspectives in Grassland
     Ecology.  Ecological  Studies. Vol.  32, Springer Verlag,  New York.  pp.
     3-24.

Lauenroth, W. K., C. J. Bleak, and J. L.  Dodd.  1979.  Sulfur Accumulation in
     Western Wheatgrass Exposed to Three Controlled  S02  Concentrations.
     Plant and Soil, 53:131-136.

Lauenroth, W. K., J. L. Dodd, and  C. E.  Dickinson.  1980.  Aboveground Biomass
     Dynamics of Blue Grama in a Short-grass Steppe  and  an Evaluation  of a
     Method for Separating Live and Dead.  J. Range  Manage.   (In press) .

Lauenroth, W. K., and J. E. Heasley.  1979.  Impact  of Sulfur Deposition on
     Grassland Ecosystems.  Symposium on Potential Environmental and Health
     Effects of Atmospheric Sulfur Deposition.  Oak  Ridge National Laboratory,
     Life Sciences Symposium Series.  14-18 October,  1979. Gatlinburg,
     Tennessee.

Lockyer, D. R., D. W.  Cowling, and L. H.  P. Jones.  1976.  A  System for
     Exposing Plants to Atmosphere Containing Low Concentrations of Sulfur
     Dioxide.  J. Exp.  Bot., 27:397-409.
                                      64

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Sokal, R. R., and F. J. Rohlf.  1969.  Biometry.  W.  H.  Freeman and  Company,
     San Francisco.  776 p.

Thomas, M. D.  1961.  Effects of Air Pollution on Plants.   In:   Air  Pollution.
     Monograph Ser. W. H. 0., No. 46 Geneva,  pp. 233-278.

Tingey, D. D., and R. A. Reinert.  1975.  The Effect  of  Ozone and  Sulfur
     Dioxide Singly and in Combination on Plant Growth.   Environ.  Pollut., 9:
     117-125.

Winner, W. E.,  and H. A. Mooney.   1980.   Ecology of S02  Resistance.  I.
     Effects of Fumigations of Gas Exchange of Deciduous and  Evergreen Shrubs.
     Oecologia.  (In Press).
                                      65

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                                    SECTION 8

                       THE IMPACT OF SULFUR DIOXIDE ON THE
                     CHLOROPHYLL CONTENT OF GRASSLAND PLANTS

                         W. K. Lauenroth and J. L. Dodd
                                    ABSTRACT

               Chlorophyll a and b contents were measured by
          extraction In ethanol for eight species native to
          northern Great Plains grasslands in North America.
          Chlorophyll a was most sensitive to S02 exposure
          but the degree of sensitivity was species specific.
          Concentrations of both chlorophylls were increased,
          unchanged or decreased depending upon S0£ concen-
          tration and species.  Chlorophyll is not a reliable
          indicator of S02 exposure in grasslands.
                                  INTRODUCTION

     Chlorophyll concentrations in plants and plant communities have been
shown to be positively related to net photosynthesis and net primary productiv-
ity (Patterson et al., 1977; Buttery and Buzzell, 1977; Brougham, 1960; Bray,
1960).  In contrast to this Ovington and Lawrence (1967) and Sanger (1971)
disputed the contention that chlorophyll concentrations and net primary
productivity were closely coupled explaining that chlorophyll expressed on
either a leaf area or dry weight basis varied widely throughout the growing
season.  Ovington and Lawrence (1967) reported dry-weight ratios of chlorophyll
to organic matter for a maize field ranged from a maximum of 19 early in the
growing season to nine late in the growing season.   Sanger (1971) suggested that
before any meaningful relationships between productivity and chlorophyll
content could be made one should be aware of the time of year and the duration
and magnitude of fluctuation of maximum chlorophyll content of the major
components of the plant community.  Although some studies have found simple
relationships between chlorophyll content and either net photosynthesis or
net primary productivity and others have not found a simple relationship,
none deny the physiological connection between chlorophyll concentration and
the potential of a plant or plant community to carry on photosynthesis.

     Chlorophyll concentration has been found to be related to many aspects
of a plant's natural environment (Sanger, 1971) as well as too many by-
products of man's activities (Knudson et al., 1977; Beckerson and Hofstraw,

                                      66

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1979; Rabe and Kreeb, 1979).  Sulfur dioxide  (S02) is an important constituent
of anthropogenic air pollution which has been shown to cause decreases in
chlorophyll concentrations over a wide range of plant species (Malhotra,
1977; Lauenroth and Dodd, submitted).  Beckerson  and Hofstraw (1979) exposed white
bean plants to concentrations of 15 pphm 862 for  5 days and found significant
increases in both chlorophyll a and chlorophyll b after 2 days exposure to
S02.  Chlorophyll a content remained higher than  the Control throughout
the 5 day period and chlorophyll b content was significantly reduced by the
end of the 5 day period.  They offered no explanation for this phenomena.
Rabe and Kreeb (1979) exposed seven different plant species to 5 pphm S02 for
approximately 1 month.  They observed non-significant decreases in chloro-
phyll content for spring grown alfalfa and for tobacco.  Significant decreases
were observed for winter barley, tulip, horsebean, turnip and alfalfa grown
in the fall.   Sulfur dioxide exposure resulted in a non-significant  increase
in chlorophyll concentration in bush tomatoes.  These responses  demonstrate
that all plants cannot be expected to respond in the same manner to  the expo-
sure of S02

     This investigation was undertaken to determine the responses of a variety
of native grassland plants to exposure to S02 under field conditions.  Previous
studies have shown that chlorophyll content of the dominant species in the
grassland, Agropyron smithii Rydb., was sensitive to exposure to S02 (Lauenroth
and Dodd,  submitted).

                             MATERIALS AND METHODS

     The chlorophyll (chl) content of actively growing stems and leaves of
eight species of grasslands plants was assessed using a modification of the
methods of Knudson et ol,, 1977 (Table  8.1).  The major modification was
substitution of a short homogenizing step in blender instead of the second
extraction.  After extraction the chopped plant material was collected on
filter paper, oven-dried and weighed.  Chlorophyll is expressed on a dry weight
basis.  Sample dates were chosen to coincide with periods of maximum vegetative
growth for each species.  Twenty-five samples of each species were collected
from each S02 treatment.  Each sample was immediately placed in a 30- ml vial
of ethanol, kept in the dark and returned to the laboratory for analysis
within 24 hours (Lauenroth and Dodd, submitted).

     Plant species selected for chl determination represented those which
were most abundant in the plant community and those with specialized functional
roles.  AgvopyTon smithO, is the dominant species in the grassland composing
40 and 60 percent of total net primary production.  Each sample of this
species consisted of three leaves.  Koeleria oristata is the second most
abundant grass in the community and each sample consisted of three leaves.
Bromus japonicus Thunb. is the most important annual grass in the plant
community and each sample consisted of six tillers each approximately 5 cm
in height.  Taraxacum offiainale is a very early  growing perennial forb and
each sample consisted of three fully expanded center leaves each approximately
7 cm in length.  Aehillea millefoliwn is another  important forb in the plant
community with a slightly later growing period than T. offioinale.   Each  sam-
ple of this species consisted of one plant with approximately three  leaves.
Sphaeraloea ooooinea  (Pursh) Rybd. is the most important forb in the community

                                      67

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TABLE 8.1-  CHLOROPHYLL CONCENTRATIONS* AND a:b RATIOS UNDER CONTROL  CONDITIONS
            AND PROBABILITIES FROM ANALYSES OF VARIANCE OF RESPONSES  OF
            CHLOROPHYLL a AND b.  LEAST SIGNIFICANT RANGES ARE  IN PARENTHESES

Statistical Results
Date
Species Sample
Psar
Spco
Trdu
Kocr
Taof
Acmi
Brja
Agsm
20
20
20
20
20
20
20
20
June
June
May
May
May
May
May
May
Chl a
4.9
3.9
3.0
5.8
6.7
2.7
15.1
4.6
Chl b
1.6
1.5
1.2
2.3
3.2
1.3
13.2
4.6
Chl a:
(control)
3
2
2
2
2
2
1
1
.0
.6
.4
.5
.1
.1
.1
.0
b
P<0
P<0
P=Q
P=0
P<0
P<0
P<0
P<0
Chl a
.001
.001
.09
.08
.001
.001
.001
.001
(0.47)
(0.65)
(- )
( - )
(1.90)
(0.22)
(4.02)
(1.27)
Chl b
P<0.001
P=0.64
P=0.02
P=0.14
P<0.001
P=0.03
P<0.001
P=0.004
(0.25)
(- )
(0.19)
( - )
(0.93)
(0.34)
(3.83)
(1.71)

  (mg
from the point of view of consumers as it is an important constituent of
diets of both antelope and cattle.  Each sample of this species was collected
from a non-flowering plant and consisted of the center three leaves.  Psoralea
argophylla Pursh is the most important legume in the community and each
sample consisted of two leaves with five leaflets each.  Tragapogon dubius is
a very common biennial forb and each sample consisted of one second year
plant.

     Statistical analysis of the data was by analysis of variance.  Tukey's Q
procedure was used to identify significant differences among treatment means
(Sokol and Rohlf, 1969).

                            RESULTS AND DISCUSSION

     The species selected for this experiment represented a wide range in con-
centrations of chl a and b (Table 8.1).   Chlorophyll a concentrations ranged
from 2.7 mg g   for Aoh-Lllea millefol-ivim to 15.1 mg g"1 for Bromus japonious.
Chlorophyll b ranged from 1.2 mg g"1 for Tragapogon dubius to 13.3 mg g"1 for
Bromus japonicus.  Ratios of chl a to b ranged from a low of 1 for Agropyron
smithii to a high of 3 for Psoralea argophylla.  Sanger (1971) reported chl a:l
ratios for three species of deciduous trees ranging from l.Q. to 3,5.  Sestak-
(1971) reviewed the literature regarding measurement of chl a and b and
                                      68

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reported that a:b ratios are generally 1.5 to 3.5.  In addition he found that
chls comprise 0.5 to  2.0 percent  of  the  dry  weight  of  plants.   Uur  results
ranged  from  0.6  to  2.8  percent.

     Exposure to S02 resulted in significant  (Table 8  .1) alterations in chl a
concentrations in six of the species examined (Figure  8  .1) and significant
changes in chl b also for six species  (Figure 8.2).  Chlorophyll concentra-
tion is often cited as a sensitive and reliable indicator of atmospheric sul-
fur dioxide  (Heck et al., 1979; Knabe, 1976; Linzon, 1978).  Our results for
chls a and b showed that a wide variety of responses may be expected.  Chloro-
phyll concentration may be a sensitive and reliable indicator of S02 exposure
in grasslands only if one carefully selects species.

     Chlorophyll contents differed among species in quantity, variability, and
response to  S02.   Koeler-ia eristata was apparently the most resistant to S02
with both chls remaining unchanged regardless of concentration.  Careful
examination  of the data indicates that chl a was decreased substantially and
chl b was decreased a small amount.  The lack of statistically significant
differences  as a result of S02 exposure was probably the result of large vari-
ability in chl content among leaves and plants.  Agropyron sm-ithii, Sphaeral-
aea aooc-inea, and Aohillea millefolium were affected with regard to chl a at
one of the S02 concentrations, but chl b remained unchanged.  Chlorophyll a
has been reported to be more sensitive to S02 than chlorophyll b (Malhotra,
1977, Peiser and Yang, 1977) although the basis for this difference is not
well documented.

     The most sensitive species we sampled was Bromus japonicus with both chl
a and b significantly reduced by the presence of S02,   Both chls were reduced
equally by the Low and High S02 treatments.  Additional indications of sensi-
tivity to S02 with respect to net production and sulfur accumulation make
this species an excellent candidate as a biological indicator of S02 air
pollution.

     The responses of three species, Psoralea argophylla, Tragapogon dubius,
and Taraxacum offioinale, were peculiar and difficult to interpret.  Chloro-
phyll a in all three species was increased by the Low  S02 treatment, unchanged
by the Medium and increased by the High treatment.  None of these changes were
significant  for T, dubius and all were significant  (P = 0.05) for the remain-
ing two species.   Chlorophyll b had the same pattern.   All changes in chl b
were significant  (P = 0.05) except the increase on the High treatment for T.
dubius.  Since our experiment was designed to document changes in chl concen-
trations as  a result of S02 exposure, we have no explanatory information for
this response.

                                 CONCLUSIONS

     Chlorophyll concentrations in grassland plants native to northern Great
Plains grasslands are not uniformly sensitive to S02 exposure.  Responses
observed for eight species ranged from significant increases to significant de-
creases.  The concept of chl ,as a sensitive and reliable indicator of S02
exposure does not hold for all species in grasslands.
                                      69

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          6.0

          5.5

          5.0

          4.5

            o'
          3.5r
       ~   3.0
        ? 2.5
                                        4.0 -
       I
       CL
       o
       cc
       o
       _l
       I
       o
10

8

6
o:
           20

           15

            10

            5

            0
     \
               %
                                    \
                              7

                              6

                              5

                              4
                              O'
                                  TREATMENTS
Figure 8.1.  Responses of  chlorophyll a to three concentrations of  862
             for;  a) Psoralea  avgophylla,  b) Spfaaevaloea oooeinea,
             c) Tragapogon dub-ius,  d) Koeleria cristata, e) Taraxacwn
             offi-Q'ina'le,   f) A.ohl11ea millefoli-um,  g) Bromus japoniaus,
             and  h) Agvopyron  srrrlthii.  Vertical bars on curves  represent
             least significant  ranges (P = 0.05).  No bars indicate no
             significant differences.
                                      70

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        E

        .Q
2.5


2.0

 1.5

  O1



 1.5

 1.3

  I.I
  0'
        I   5.5
        D.
        O
        CC   4. K.
        O   ^-S

        o   3.5
            2.5
 0


2.5

2.0

 1.5
                                            T
                              0.9
            20 -

             15 -

             10 -

             5

             0



                                     TREATMENTS
Figure 8.2.    Responses of chlorophyll b  to  three concentrations of SC»2
               for;   a)  Psovalea argophylla,   b)  Sphae-palcea oocei-nea.,
               c)  Tvagapogon dubius, d) Koeleria  or-Lstata,  e) Taraxacum
               offioinale,  f) Aehillea millefoliien,   g)  Bromus japon-Lcus,
               and  h) Agropyron snrithii.  Vertical bars  on curves represent
               least significant ranges  (P =  0.05).  No bars indicate no
               significant differences.
                                       71

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                                 REFERENCES

Beckerson,  D.  W.,  and G.  Hofstra.  1979.   Effect  of  Sulfur Dioxide and Ozone
     Singly or in Combination on Leaf  Chlorophyll, RNA  and Protein in White
     Bean.   Can.  J.  Bot., 57:1940-1945.

Bray, J. R.  1960.  The Chlorophyll Content  of  some  Native and Managed Plant
     Communities  in Central Minnesota.  Can.  J. Bot., 38:313-333.

Brougham, R. W.  1960.  The Relationship  Between  the Critical Leaf Area,
     Total Chlorophyll Content and Maximum Growth Rate  of some Pasture and
     Crop Plants.   Ann. Bot.,  24:463-474.

Buttery, B. R., and R. I. Buzzell.   1977.  The Relationship Between  Chloro-
     phyll Content and Rate of Photosynthesis in  Soybeans.  Can. J.  Plant
     Scl.,  57:1-5.

Heck, W. W., S. V. Krupa, and S.  N. Linzon.   1979.   Methodology for  the
     Assessment of Air Pollution Effects  on Vegetation.  APCA Specialty Con-
     ference Proceedings.  April 19-21, 1978, Minneapolis, Minnesota.

Knabe, W.  1976.   Effects of Sulfur Dioxide  on Terrestrial Vegetation.
     Ambio., 5:213-218.

Knudson, L. L., T. W. Tibbets, and G.  E.  Edwards.  1977.  Measurement of
     Ozone Injury by Determination of  Leaf Chlorophyll  Concentration.  Plant
     Physioi., 60:606-608.

Lauenroth,  W.  K.,  and J.  L. Dodd.  Chlorophyll Reduction in Western  Wheatgrass
     Exposed to Sulfur Dioxide.   (Submitted)  Water, Air and Soil Pollut.

Linzon, S.  N.   1978.  Effects of Airborne Sulfur  Pollutants on Plants.  PP '
     110-162 In:   J. 0. Nriagu (ed.) Sulfur  in  the Environment; Part II.
     Ecological Impacts.   John Wiley and  Sons,  Inc., New York.

Malhotra, S. S.  1977.  Effects of Aqueous Sulfur Dioxide on Chlorophyll
     Destruction in P-inus contorta. New  Phytol., 78:101-109.

Ovington, J. D.,  and-D. B.  Lawrence.   1967.   Comparative Chlorophyll and
     Energy Studies of Prairie,  Savannah,  Oakwood and Maize Field Ecosystems.
     Ecology,  48:515-524.

Patterson,  D.  T.,  J. A. Bunce, R. S. Alberte, and E. Van Volkenburgh.  1977.
     Photosynthesis in Relation to Leaf Characteristics of Cotton from Con-
     trolled and Field Environments.   Plant  Physioi., 59:384-387.

Peiser, G.  D., and S. F.  Yang.  1977.  Chlorophyll Destruction by the Bisulfite-
     Oxygen System.   Plant Physioi., 60:277-281.

Rabe, R., and K.  H.  Kreeb.   1979.  Enzyme Activities and Chlorophyll and Pro-
     tein Content in Plants as Indicators of  Air  Pollution.  Environ. Pollut.,
     19:119-137.

                                      72

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Sanger, J. E.  1971.  Quantitative Investigations  of  Leaf Pigments from Their
     Inception in Buds, Through Autumn Coloration,  to Decomposition and
     Falling Leaves.  Ecology, 52:1075-1089.

Sestak, Z.  1971.  Determination of Chlorophylls a and b.   PP • 672-701, In:
     Z. Sestak, J. Catsky, and P. G. Jarvis (eds.), Plant Photosynthetic Pro-
     duction:  Manual of Methods.  Dr. W.  Junk, N.V., Publishers, The Hague,
     818 pp.

Sokal, R. I., and F. J. Rohlf.  1969.  Biometry.   W.  H.  Freeman and Co., San
     Francisco.  776 pp.
                                      73

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                                  SECTION 9

           ADHERENCE OF WATER TO LEAF SURFACES OF AGROPYRON SMITEII

                           J. L. Dodd and J.E. Heasley


                                   ABSTRACT

               Leaf blades of live western wheatgrass wer~e
          immersed in room temperature water to determine an
          upper limit for water adherence to blade surfaces.
          A reasonable value for adherence of water to these
          surfaces was ca. 50 mg • dm~2.



                                 INTRODUCTION

     The purpose of this short communication is to document results of a
limited investigation designed to determine the approximate maximum quantity
of water that will adhere to live external leaf surfaces of Agropyron smithii
Rydb.  Results of the investigation will be incorporated into a mathematical
model that simulates the flux of S02 to external and internal surfaces of
western wheatgrass blades.  Since the flux rate of S02 to external leaf sur-
faces varies, in part, with the amount of water adhering to blade surfaces
it is necessary to know a maximum value to simulate flux rates immediately
following rainfall and dew events.

                             MATERIALS AND METHODS

     We utilized leaf tissue from well watered and fertilized potted plants
reared in the greenhouse.  Blade portions of leaves were separated into three
equal segments — base, mid-portion, and tips.  Each segment varied from
70-90 mm, depending on overall length of blade.

     The 32 blade sections of each class were clipped from the living plant,
weighed Immediately, immersed in distilled water, and reweighed to determine
mass of adhered water.  Visible droplets of water were shaken from blade seg-
ments before reweighing.  Length and width of blade segments were then measured
to the nearest mm for determination of leaf area.  Adhered water was expressed
as mg • dm~2 (both surfaces).
                                      74

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                            RESULTS AND DISCUSSION

     The basal and mid-portions of live western wheatgrass leaves appear to
have a lower capacity to adsorb water than do the tips of leaves (Table  9.1)
However, it is possible that this difference is due, at least in part, to
underestimating the area of blade tips by assuming that they were triangular
in shape.  Subsequent examination of other Agropyron smifhii blades indi-
cated that leaf tips are not always perfectly triangular but are sometimes
parallel for a portion of their length and begin to converge to a point
within 10-20 mm of the end of the blade.

                                   CONCLUSION

     We conclude that the estimates of 58 and 45 mg •  dm~2 (approximately
50 mg • dm~2) are the most appropriate estimates to be used as an upper limit
for the adherence of water to live western wheatgrass  blades.  This estimate
of adherence, of course, does not include water trapped on blades in large
droplet form as might occur on in situ plants in the field.  Water collected
on blades in this form would be dependent upon plant morphology, precipita-
tion form, wind speed, and canopy architecture, and falls outside the scope
of this limited investigation.
          TABLE  9.1.  ADHERED WATER (X ± SE) ON SURFACES OF LIVE
                       LEAF BLADES OF Agropyron smithii
            Base                    Middle                       Tip

          mg • dm~2               mg • dm~2                   mg •  dm~2
           58 ±10                 45 ± 11                    128 ± 28
                                      75

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                                 SECTION 10

         THE INFLUENCE OF PRECIPITATION ON THE SULFUR CONCENTRATION OF
               AGROPIRON SMITEII RYBD.  EXPOSED TO SULFUR DIOXIDE

         D.  G.  Milchunas, J.  L.  Dodd, J. E. Heasley,  and W.  K.  Lauenroth
                                    ABSTRACT

               The leaching by rain of S02  deposited sulfur from
          AgTOpyvon smifh-i-i tillers in a semi-arid Montana grassland
          exposed to 7.7 pphm S02  was estimated to be less than
          from 5 to 13 percent depending on the time of exposure.
          Accounting for intensity and frequency of rainfall in
          addition to duration of  S02 exposure increased our ability
          to predict live plant sulfur concentration by 6 percent.
          Sulfur accumulation in live plants was linear up until
          the time of senescence.   Overwinter losses of plant sulfur
          were estimated to be 54  and 74 percent for control and
          S02 exposed Agropyron smithi-i- tillers, respectively.
                                  INTRODUCTION

     The removal of S02 from the atmosphere by plants occurs by adsorption onto
external leaf surfaces and by absorption via diffusion through the stomata
followed by dissolution of the gas in the water film coating the walls of the
sub-stomatal chamber.   Sulfur dioxide absorbed by the plant can cause disrup<-
tion of various metabolic processes when the resulting concentrations of sul-
fur compounds exceed maintenance and growth requirements.   Sulfur on the sur-
face of the plant is not involved in plant metabolism.

     Studies attempting to distinguish between adsorption and absorption of
S02 in plants have involved washing or soaking of the exposed plant parts to
separate the two fractions.  Utilizing plants exposed to 35S02, Garsed and
Read (1977) soaked the leaves twice for 45 minutes with gentle shaking to ob-
tain a leachate which  contained 15 to 38 percent of the total 35S02-  A 20 to
25 percent reduction in sulfur was obtained by Rice et al.  (1979) for plant
parts exposed to S02 then placed in a screened jar and rinsed with rapidly
flowing tap water for  3 minutes.   Values obtained in this manner over-
estimate surface deposition or even the leaching of sulfur  by natural rainfall
events.
                                      76

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     That rainfall leaches internal substances from plants is well documented,
and this topic has been reviewed by Tukey and Tukey (1962) and Tukey (1970) .
The ease with which internal compounds are leached from plants make it diffi-
cult to experimentally discern between absorption and adsorption of S02.
Data from one study which measured stomatal S02 absorption versus total S02
deposition to plant leaves showed little adsorption by Ee^eromeles arbutifolia
and greater adsorption by Diplaous aurantiaous because of it's very sticky
leaves (Winner and Mooney, 1980).  Considering that; 1) sulfur can accumulate
to very high concentrations in plants exposed to S02 (Lauenroth et al.,
1979), 2) rainfall can leach considerable internal quantities of substances
from plants (Tukey, 1970), and 3) sulfur in plant tissues is classified as
moderately leachable (Tukey et al., 1958), the amount of sulfur removed by
rainfall may be of more biological importance than the commonly used distinc-
tion between external and internal sulfur implies.

     This study investigated the effect of rainfall on sulfur concentrations
of live and dead western wheatgrass (Agropyron smithii Rydb.) tillers growing
in a native Montana grassland exposed to a controlled level of S02 .

                            MATERIALS AND METHODS

     Four live and four last year's dead Agropyron smithi-i, tillers were col-
lected each morning during July, August, and September from fixed locations
 on Control and High treatment plots.     Daily precipitation was recorded to
the nearest tenth of a millimeter at the time of sampling.  Total sulfur
concentrations of the oven dried (60°C) plant material were assessed with a
Leco Induction Furnace (Jones and Isaac, 1972).

     Julian date and four variables descriptive of the precipitation events
were utilized in stepwise multiple regression analysis to determine their
relationships with sulfur content.  The four variables used to describe
rainfall events were:  1) Total5 = total rainfall in the previous 5 days,  2)
#/5 = number of rain days in the previous 5 days, 3) day last = day number
of last rain event, and 4) amount last = amount of rain in last rain event.

                            RESULTS AND DISCUSSION

     Precipitation totaling 55 mm occurred on 14 out of 77 days during the
course of this study.  This was relatively low compared to the 20 year
mean of 88 mm for July, August and September in Billings, Montana.  The
largest rainfall 'event was 19 mm on 29 July.

     Julian date was the best single predictor (r2 = 0.68) of sulfur content
for live Agropyron smithii tillers exposed to S02 (Table 10.1).  Accounting
for total rainfall in 5 days preceding a sampling date increased prediction.
capabilities to 0.70.  The use of Julian date and three additional rain event
variables increased the coefficient of variation by only 6 percent.  No sig-
nificant relationships were found for sulfur concentrations in S02-dead,
Control-live,  or Control-dead material.

     Calculations were made to determine to what degree plant sulfur levels
would have had to decline after a rain event in order to have statistically


                                      77

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 TABLE  10.1.  COEFFICIENTS OF DETERMINATION FOR FIVE VARIABLES UTILIZED  TO  PRE-
             DICT SULFUR CONCENTRATION IN LIVE Agropyron smithii PLANTS EXPOSED
             TO 7.7 PPHM S02.*
                VARIABLE                                     r£

 J-date                                                    .6778

 J-date,  total5                                             .6961
 J-date,  #/5                                                .6804
 J-date,  day  last                                           .6801
 J-date,  amount  last                                        .6780

 J-date,  amount  last,  tota!5                                .7145
 J-date,  total5, #/5                                        .7003
 J-date,  totals, day  last                                   .6961
 J-date,  amount  last,  #/5                                   .6811
 J-date,  #/5,  day  last                                     .6807

 J-date,  amount  last,  tota!5, #/5                           .7361
 J-date,  amount  last,  total5, day last                      .7324
 J-date,  total5, #/5»  daY  last                              .7024
 J-date,  amount  last,  #/5, day last                         .6812
     The five variables are Julian date  (J-date),  the  total  rainfall  in  the
     previous 5  days  (Totals),  tne number  of  rain  days in the previous
     5  days  (#5),  the  day  number  of  the  last  rain  event (Day Last),  and
     the amount  of  rain in the  last  rain event  (Amount Last).
detected a leaching effect.  Confidence bands  (95 percent) were formulated about
the regression of sulfur concentration on date for S02-live data.  Rain would
have had to have leached 13, 5, and 8 percent of the sulfur content of live
plants exposed to S02 on early, middle, and late sampling dates, respectively,
for data points to have fallen outside the 95 percent confidence bands.

     Sulfur concentrations in live Agropyron smithii tillers on the S02
treatment increased through the growing season to a peak in late August;
after which they declined (Figure 10.1).  A comparison between early and peak
sulfur concentration was made by an analysis of variance on the first seven
data points and seven consecutive late August data points.  Sulfur concentra-
tion increased 43 percent (p = 0.037) in control-live and 69 percent (p =
0.001) in S02-live plants.  Sulfur concentrations of last year's dead tillers
increased 35 and 24 percent (p = 0.002 and 0.001) for control and S02 treat-
ments, respectively.  Estimates of overwintering decreases in sulfur concen-
tration were made by comparing peak live with early season dead sulfur


                                      78

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   0.4
   0.3
O


<

tr
o
o
o
CO
   0.2
    O.I
                       '
                                                                          /\
                                                                     /I /    XB
                                                                     /  "
                                                                     •  w
                          JULY
                                                               AUGUST
           SEPTEMBER
Dates
                                    o
                                    
-------
concentrations.  These estimates suggest that overwinter losses were 54 and
74 percent (p = 0.001 and 0.036) on the control and S02 treatment ,  respec-
tively.

     In addition to leaching, precipitation can potentially affect the dis-
tribution of sulfur in a system exposed to SC>2 through its effect on atmos-
pheric S02 and by increasing surface deposition because of the high solubility
of S02 in water (Hocking and Hocking, 1977; Terraglio and Manganelli, 1967).
We could not detect increases in the sulfur concentration in ground level
dead Agropyvon smifhii tillers after rainfall events.  It must be stressed,
however, that this study was conducted in a semiarid grassland habitat in a
below average rainfall year.  In Alberta, Canada, Nyborg et al. (1977) reported
that rain intercepted by forest trees exposed to S02 had a sulfur content 3
to 4 times greater than rain that was not intercepted.

     During the wet season in the tropics, the growth and yield of plants may
be severely limited by the inability of their roots to absorb and replace
nutrients in sufficient quantities to overcome losses via leaching (Tukey,
1970).  On the other hand, leaching can be an excretion process by which
waste products and substances in excess of requirements can be elimited
(Franke, 1967; Stenlid, 1958).  The physiological process of guttation through
hydathodes and the high salt content of the excreted fluid has been recognized
for a long time (Curtis, 1943; Greenhill and Chiball, 1934).  The possible
function of guttation and leaching in avoidance of S02 injury by plants in
wet climates warrants further investigation.  Guttated fluids can be washed
away by rain or be drawn back into the plant (Curtis, 1943).  Considering
that guttation in dry habitats usually occurs at night when S02 concentrations
are highest,  and that S02 deposition is greatly increased on wet surfaces
because of the high solubility of S02 in water, guttation in dry climates
where leaching is not as important of a factor as in wet climates may actually
increase S02 uptake and constitute another route of entry of sulfur in plants.

     Seasonal peak plant sulfur concentration did not coincide with peak
plant growth  (Dodd et al. ,   1980).  Milchunas  et al. (In Prep.) observed a
peak in Agropyvon smifhii live leaf area in late June - early July, whereas
peak sulfur concentrations occurred in late August.  Data from this study and
Lauenroth et al. (1979) indicates that sulfur accumulation in live plants
exposed to S02 is linear throughout the growing season.  The high overwinter
loss of 54 and 74 percent sulfur for Control and S02 exposed tillers, respec-
tively, occurs as cell walls deteriorate and their contents leach.  The
following year, sulfur content of the dead material increased.  Gosz et al.
(1976) observed an initial period in litter decomposition when the relative
abundance of carbon to minerals was lowered by microbial oxidation.  The
smaller increase in the sulfur concentration of dead Agvopyvon smithii tillers
on the S02 treatment may be a reflection of decreased decomposition rates
with S02 exposure (Dodd and Lauenroth, 1980),

                                  CONCLUSIONS

      The  leaching by  rain of  sulfur  from Agropyron smithii  tillers in a  semi-r
arid  Montana  grassland  exposed  to  7.7  pphm S02 was estimated  to be less  than
5  to  13 percent depending on  the  duration of exposure.  Accounting for the

                                      80

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 intensity and frequency of rain in addition to the duration of S02 exposure
 increased the ability to predict live plant sulfur concentration by 6 per-
 cent.   Sulfur accumulation in live plants was linear throughout the growing
 season (r  = 0.68).   Overwinter losses of plant sulfur were estimated to be
 54 and 74 percent for control and S02 exposed Agropy Ton smithii tillers,
 respectively.  The following spring,  sulfur content of dead Agropypon sm-Lthii
 increased through the summer as microbial decomposition reduced organic carbon
 to mineral ratios.

                                   REFERENCES

 Curtis,  L.  C.  1943.   Deleterious Effects of Guttated Fluids on Foliage.  Am.
      J.  Bot., 30:778-781.

 Dodd,  J.  L.,  and W.  K.  Lauenroth.  1980.   Effects of Low-level S02 Fumigation
      on Decomposition of Western Wheatgrass Litter in a Mixed-grass Prairie.
      In:   E.  M.  Preston and D.  W. OfGuinn (eds.)   The Bioenvironmental Impact
      of a Coal-fired Power Plant, Fifth Interim Report, Colstrip,  Montana.
      EPA-600/3-80-052.   U.S.  Environmental Protection Agency,  Corvallis,
      Oregon.   In Press.   pp.  212-215.

 Dodd,  J.  L., W.  K. Lauenroth, and R.  K. Heitschmidt.    1980.  Effects of
      Controlled S02 Exposure on Net Primary Production and Plant Biomass
      Dynamics.  In:  E.  M.  Preston and D.  W. O'Guinn (eds.)  The Bioenviron-
      mental Impact of a Coal-fired Power Plant, Fifth Interim Report,  Colstrip,
      Montana. EPA-600/3-80-052. U.S.  Environmental Protection Agency,
      Corvallis,  Oregon. In Press,  pp. 172--184.

 Franke, W.  1967.  Mechanisms of Foliar Penetration of Solutions.   Ann. Rev.
      Plant Physiol., 18:281-300.

 Garsed, S. G., and D. J. Read.  1977.  The Uptake and Metabolism of 35S02 in
      Plants of Differing Sensitivity to Sulphur Dioxide.  Environ. Pollut.,
      13:173-186.
 Gosz, J. R., G.  E. Likens, and F. H.  Bormann.  1976.  Organic Matter and
      Nutrient Dynamics of the Forest and Forest Floor in the Hubbard Brook
      Forest.  Oecologia, 22:305-320.

 Greenhill, A.  W.,  and A. C. Chiball.   1934.   The  Exudation of Glutamine  from
     Perennial Rye-grass.  Biochem. J., 4:1422-1427.

 Hocking, D.,  and M. B. Hocking.   1977-  Equilibrium Solubility  of Trace  Atmos-
     pheric Sulfur Dioxide in Water and its Bearing on Air Pollution In-jury
     to Plants.  Environ. Pollut., 13:57-64.

Jones, J. B., and R. A. Isaac.  1972.   Determination of Sulfur  in Plant
     Material Using a Leco Sulfur Analyzer.  J. Agr. Food Chem., 20:1292-1294.

Lauenroth, W. K., C. J. Bicak, and J.  L. Dodd.  1979.   Sulfur Accumulation in
     Western Wheatgrass Exposed to Three Controlled S02 Concentrations.
     Plant and Soil, 53:131-136.
                                      81

-------
Milchunas, D. G. , W. K. Lauenroth, and J. L. Dodd.  In Prep.  Effects of S02
     Exposure with Nitrogen, and Sulfur Fertilization on the Growth of
     Agropyron smithi-i- Rybd.  In:  E. M. Preston, D. W. O'Guinn, and R. A.
     Wilson  (eds.)  Bioenvironmental Impact of a Coal-fired Power Plant,
     Sixth Interim Report, Colstrip, Montana.  U. S. Environmental Protection
     Agency, Corvallis, Oregon.

Nyborg, M., J. Crepin, D. Hocking, and J. Baker.  1977.  Effect of Sulphur
     Dioxide on Precipitation and on the Sulphur Content and Acidity of
     Soils in Alberta, Canada.   Water, Air, and Soil Pollut., 7:439-448.

Rice, P. M., L. H. Pye, R. Boldi, J. O'Loughlin, P.  C.  Tourangeau, and C.  C.
     Gordon.  1979.  The Effects of "Low Level S02"  Exposure on Sulfur Accumu-
     lation and Various Plant Life Responses of Some Major Grassland Species
     on the ZAPS Sites.  In: E. M. Preston and T. L. Gullett (eds.)  Bio-
     environmental Impact of a Coal-fired Power Plant,  Fourth Interim
     Report, Colstrip, Montana. EPA-600/3-79-044. U.S.  Environmental Protection
     Agency, Corvallis, Oregon, pp. 494-591.

Stenlid, G.  1958.  Salt Losses and Redistribution of Salts in Higher Plants.
     Encycl. Plant Physiol., 4:615-637.

Terraglio, F. P., and R. M. Manganelli.  1967.  The Absorption of Atmospheric
     Sulfur Dioxide by Water Solutions.  J. Air Pollut. Control Assc., 17:403-
     406.

Tukey, Jr., H. B.  1970.  The Leaching of Substances from Plants.  Ann. Rev.
     Plant Physiol., 21:305-324.

Tukey, Jr., H. B., and H. B. Tukey, Sr.  1962.  The Loss of Organic and In-
     organic Materials by Leaching from Leaves and Other Above-ground Plant
     Parts,  In:  Radioisotopes in Soil-Plant Nutrition Studies, Proceedings
     IAEA, Vienna,  p. 289-302.

Tukey, Jr., H. B., H.  B. Tukey, Sr., and S. H. Wittwer.  1958.  Loss of
     Nutrients by Foliar Leaching as Determined by Radioisotopes.  Proc. Am.
     Soc. Hort. Sci.,  71:496-506.

Winner, W. E. and H. A. Mooney.  1980.  Ecology of S02  Resistance:  II.
     Photosynthetic Changes of Shrubs in Relation to S02 Absorption and
     Stomatal Behavior.  Oecologia, 44:296-302.
                                     82

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                                  SECTION 11

            SULFUR DISTRIBUTION AND ALLOCATION IN WESTERN WHEATGRASS
              EXPOSED TO S02 UNDER VARIABLE NUTRIENT SULFUR REGIMES

                  C.  J.  Bleak,  W.  K. Lauenroth,  and  J.  L. Dodd
                                  ABSTRACT

               Sulfur concentrations in western wheatgrass  plants
          were measured in shoots and roots,  individual leaves,
          and leaves subdivided into three blade segments.   Plants
          were exposed to Control or High S02 and were main-
          tained in hydroponic solutions without sulfur,  and at
          both optimum (2 mM)  and double the  optimum (4 mM)  con-
          centration of sulfur.  Leaf tips contained more sulfur
          than middle or basal blade segments and fumigated leaves
          contained more sulfur than unfumigated leaves.  Added
          S02 did not alter the sulfur contents of either
          shoots or roots.  However, added sulfur in the  nutrient
          medium increased root and shoot sulfur levels.  Shoot-
          root biomass ratios were greater in fumigated plants
          in the early season.  Late in the season however,  dif-
          ferences due to S0£ fumigation were not discernible.
                                  INTRODUCTION

     With the rapid development of coal mining and associated coal-fired
power plants in the western states,  the impact of air pollutants on grassland
ecosystems has become of considerable importance (Preston and Gullett,  1979) .
Cool season grasses make up the predominant vegetation cover of prairies in
coal-producing regions of southeast Montana and are an important component of
the diet of both wild and domestic herbivores.  While many investigations
have centered upon plant responses to S02 under laboratory conditions,  few
studies have utilized field exposures.  Laboratory fumigation trials rarely
simulate ambient fluctuations in S02 concentration and present problems in
extrapolation to field conditions.  The objective of this study was to  deter-
mine the interactive effects of atmospheric and substrate S on sulfur metabo-
lism of a GS grass native to mixed prairies in southeast Montana.  Emphasis was
placed upon sulfur distribution and allocation in western wheatgrass as well
as alterations in the relative masses of shoots and roots.
                                     83

-------
     Many  reviews have recognized sulfur dioxide injury to vegetation  (Jacobson
 and Hill,  1970; Wolozin and Landau, 1966), but researchers have only recently
 begun  to examine the physiological alterations and the subsequent fate of S02
 in the plant system (Malhotra and Hocking, 1976; Ziegler, 1975).  Sulfur
 distribution and allocation in native plants have not been fully characterized
 and the nutrient has often been considered relatively immobile once an optimal
 leaf sink  concentration has been achieved (Salisbury and Ross, 1978; Latichli,
 1972).  Optimal sulfur concentrations have been suggested to range from 1500
 pg • g"1 to 3000 pg • g"1 in forage grasses (Metson, 1973) .  Plants in an
 atmosphere containing measurable levels of S02 may be subjected to a physio-
 logical stress as the sulfur concentration in the tissue approaches some
 toxic  level.  Tingey e~b al. (1978) found that western wheatgrass was relative-
 ly resistant to S02 with concentrations greater than 100 pphm required to
 induce visible injury.  Even though visible injury may be minimal, sulfur
 levels greater or less than an optimal level may induce severe physiological
 stress upon a plant.  Malhotra and Hocking (1976) have reviewed current
 physiological literature and have noted inhibitory effects of S02 on plants
 that include interference with photosynthetic C02 fixation and a reduction in
 the buffering capacity of plant cells.  It is conceivable then, that such
 subtle shifts in whole plant sulfur status may imply long-term alterations in
 the mixed-prairie ecology.

     Plant sulfur content and partitioning are not well characterized under
 S02 fumigation conditions in the field.  The focus of this paper is upon this
 problem.   In light of the foregoing discussion the following objectives have
 been established in this study;  1) determine the role of deficient and
 excess nutrient sulfur levels in conjunction with S02 in affecting changes in
 sulfur distribution and accumulation in western wheatgrass,  2) determine the
 relative mobility of sulfur in western wheatgrass, 3) determine potential
 plant  tissue sinks for sulfur.

                              MATERIALS AND METHODS

 Experimental Design

     To provide a nutrient system that would allow precise manipulation of
 sulfur concentration, hydroponic containers were employed.  Extensive re-
 search has been conducted with hydroponic systems and cultivated species such
 as tomatoes and cucumbers (Salisbury and Ross, 1978) while concern for native
 vegetation has been limited.  Although some work with native grasses and
 nutrient solutions has been reported in the literature (Williams and Kemp,
 1978;  Detling et al., 1979) most of this has focused upon photosynthetic re-
 sponses to changing environmental conditions.


     Western  wheatgrass  (.Agropyron smithii Rybd.)  plants  were  grown in hydro-
ponic culture with  a full  complement  of elemental nutrients  in one-seventh
strength solution as described by Hoagland and Arnon (1938).   Containers  held
approximately 8  liters  and adequately sustained 24 plants.   Upon transfer
from the greenhouse to  the fumigation site in Montana,  plants  were moved  to
4 liter styrofoam containers with eight plants per container.   Containers
were  covered  and taped  to  minimize deposition of  S02 to  solution surfaces.


                                      84

-------
     Two experimental periods were selected during the growing season.  The
first progressed from June 20 to June 26, 1979  (147 hours) while the second
progressed from August 12 to August 18, 1979 (147 hours).  These time intervals
coincided roughly with periods of maximal photosynthetic rates and 50 percent
senescence respectively, in native western wheatgrass plants in situ.  Develop^
mental stages were similar in greenhouses-grown  and in situ plants in the spring.
In the early season, four experimental containers were placed on each of the
Control and SC>2^fumigated plots.  Nutrient sulfur concentrations were varied
such that one container received no sulfur, one received complete sulfur (2
mM), and one received double (4 mM) the complete sulfur complement.   A fourth
container held eight dry western wheatgrass plants.  These plants were not
physiologically functional and were included in the design to simulate senes-
cent leaf material in which the predominant sulfur input would be surface de-
position.  The late season trial was similar in design to the early season
trial but greenhouse-grown plants were in an earlier developmental stage than
in situ plants.

Plant Analysis

     Plant material was oven-dried at 60°C to a constant weight.  Sulfur
content of leaves, shoots, and roots was assessed in all plant material in
hydroponic containers across all S02 fumigation plots.  At the time of harvest,
plants were divided into shoot and root components to prevent potential
subsequent sulfur translocation.  Some individual blades were further divided
into leaf blade tips, midsections, and bases each approximately 6 cm long.
Sulfur content (mg S/mg tissue) was measured with a LEGO Induction Furnace
(Laboratory Equipment Corporation, St. Joseph, Michigan, USA) with the inor-
ganic sulfate ion (SOf) the primary form of sulfur recovered.  Data were
subjected to analyses of variance to discern any treatment differences while
means reported include standard errors about them.

                             RESULTS AND DISCUSSION

     Most gaseous pollutant investigations have focused upon responses of
dicots, particularly cultivated species (Jacobson and Hill, 1970; Guderian,
1977).  Since the growth and development of grasses are notably different
(Esau, 1965), extrapolation of responses to air pollutants from one form of
growth to another may not be valid.  Development of dicots is characterized
by leaf expansion in the light, whereas a specialized leaf unrolling process
occurs in grasses (Leopold and Kriedemann, 1975) which results in a gradient
in the functional age of individual grass blades.  Development of grasses
proceeds from the crown with older leaves near the base and younger leaves
near the tip of the plant.  Individual leaf initiation and expansion occurs
such that the leaf tip is the oldest and the base the youngest portion of the
leaf (Langer, 1972).  Since there is a difference in the development of
grasses and dicotyledonous species it may be assumed that patterns in plant
sulfur content and distribution may also be very different.  To better under-
stand the impact of coal-fired power plants upon mixed-prairie vegetation,
research efforts must concentrate upon endogenous grass species.  This paper
focuses upon comparisons of plant material exposed under control conditions
(-S02) and with S02 fumigation (7.7 pphm) as well as comparisons between
plants grown in different S-nutrient solutions.  Sulfur distribution and


                                      85

-------
allocation are discussed below with consideration of three levels of organiza-
tion; 1) segments of leaf blades, 2) whole leaves, and 3) whole plants.

Leaf Segments

     Sulfur content in segments of the leaf blade was significantly different
(P < 0.01) in both the early and late exposure periods of the growing season
with the highest sulfur levels in the oldest portion of the grass blade  (tip)
and the lowest sulfur levels in the youngest portion of the blade (base).
The gradient in blade sulfur content from oldest to youngest tissues was
consistent with and without S02 fumigation (Figure 11.1).  While there was no
significant interaction between S02 exposure level and the sulfur content of
individual parts of the blade, the data and the evidence of Lauenroth e~k al.
(1980)  lead  us to believe that sulfur levels were higher in leaf blade
parts from unfumigated plants than from fumigated plants.  Gradients in  sulfur
content between tips and bases were also reported by JMger (1976) , utilizing
spruce needles exposed to S02.  Guderian (1977) suggested the secondary
transport of sulfur taken up as S02 to blade tips and margins as an explanation
for this gradient.  Although JMger (1976)  and Guderian (1977) both cite
Halbwachs (1963) to explain this transport via the movement of sulfate in
water and an associated water potential gradient toward tips and margins, it
is conceivable that tips are simply exposed for a longer period of time and
accumulate more sulfur than the younger portion of the blade.  Lower sulfur
levels in parts of the blade from fumigated plants suggest that a translocation
mechanism may be implicated in plants exposed to S02 that shunts sulfur from
                      0.5
                    en
                    £ 0.4

                    g
                    K
                      0.3
                    o
                    o
                      O.I
                          Tip
                                   Mid
                                  LEAF PART
                                              Base
Figure 11.1.
Sulfur content in segments of the leaf blade following late
season exposure.  	(- 862) 	  (+ S02).
                                      86

-------
foliar parts to roots more readily than when the ambient atmospheric sulfur
levels are negligible.  That is, the sulfate sulfur concentration gradient
between shoots and roots is steepened.  Such a transfer however, does not
necessarily imply an increase in biomass (Table 11.1).  According to Munch
(1926), solute concentration at a source (i,e., shoot) may dictate the rate
and bulk flow of that solute to a sink (i.e, , root).   Ionic transfer may be
similar as downward movement of sulfate sulfur through phloem tissue is
accelerated.  Rennenberg et al. (1979), working with tobacco, presented
evidence that reduced sulfur, with S02 as its source (Garsed and Read,
1977), is translocated from leaves to roots.

     Differences in the sulfur content of segments of leaf blades were also
related to variations in nutrient solution sulfur (Figure 11.2).  Sulfur
content varied only with blade segment (P 1 0.01) and not sulfur nutrition
with results similar with and without S02 fumigation.  Although the effects
of nutrient solution treatments upon the sulfur content of parts of the blade
were not significantly different from one another, the trend suggests consis-
tently greater blade segment sulfur content when the nutrient solution contains
twice the optimal level.  These data also support the idea of a leaf tip to
base gradient in sulfur concentration.  Differences in sulfur content among
the three nutrient solutions were smallest in leaf bases.  Accumulation of
sulfur in plant material kept in high sulfur nutrient solutions  may be ex-
plained by a more traditional translocation mechanism than may operate when
S02 is a primary controller or regulator of sulfur distribution.  Sulfate is
TABLE 11.1. SHOOT-ROOT BIOMASS RATIOS FOR WESTERN WHEATGRASS PLANTS WITH AND
            WITHOUT S02 AND WITH THREE NUTRIENT SOLUTION SULFUR LEVELS *
     Early Season  (s/r)
t
A no S
D no S

1.13
1.83

No difference
(P = 0.12)
                              Late Season  (s/r)
A no S
D no S
1.62
2.16
No difference
(P = 0.17)
A comp S 2.14
D comp S 2.21

A doub S 1.48
D doub S 1.63
No difference
   (P = 0.41)

No difference
   (P = 0.35)
A comp S 2.39
D comp S 2.21

A doub S 1.60
D doub S 2.38
No difference
   (P = 0.41)

No difference
   (P = 0.14)
A dep
D dep
0.86
0.88
No difference
(P = 0.47)
A dep
D dep
1.26
0.78
No difference
(P = 0.12)

     Two sample T-tests indicated no significant difference (P 1 0.05)  between
     the two fumigation plots among four nutrient solution treatments,  across
     two time periods in the growing season.

     A = (- S02)
     D = (+ S02)
                                      87

-------
                          0.6 -
                          03 -
                          0.2
Figure 11.2.
Sulfur content in segments of the leaf blade following late
season exposure.   	 No S solution
 	  Complete S solution	Double S solution .
translocated from roots to the leaves through the transpiration stream.  In
this way the excess sulfur load to which roots are exposed, may be alleviated.
Early and late season data were similar.

Whole Leaves

     Statistical analysis of the sulfur content of whole leaves indicated
significantly (P < 0.05) greater sulfur in leaves exposed to 7.7 pphm SC>2
than in unexposed plants for all the nutrient solution treatments in the
early season (Figure 11.3).  In contrast to this, sulfur content in whole
leaves of fumigated plants across the nutrient solution treatments was signi-
ficantly less (P ^ 0.05) than with no fumigation in the late season with
difference due primarily to enhanced sulfur levels with the complete sulfur
solution (Figure 11.4).  To examine this apparent anomaly in more detail,
data were subjected to a three way analysis of variance, including each of
four leaf ages, with the 862 and nutrient solution sulfur information.
Differences in sulfur content were not significant among leaves of different
developmental or physiological ages.  We suggest that the 147 hour exposure
interval is insufficient in both the early and late periods of the season to
identify trends in plant sulfur distribution for all leaves combined or on an
individual leaf age basis.
                                      88

-------
Figure 11.3.
                        0.4
                     IT
                     H  0.3

                     LU
                     O
                     2
                     O
                     O

                     tr
                        0.2
                     CO
             No S      Complete S    Double S


              NUTRIENT SOLUTION  SULFUR

Sulfur content in whole leaves  following early  season exposure,
	(_  S02)  	  (+ S02) .
                            0.4
                          g

                          5
                          I 0.3
                            0.2
                                 No S      Complete S    Double S

                                  NUTRIENT  SOLUTION SULFUR
Figure 11.4.
Sulfur  content in whole leaves  following late season exposure,

	(_  S02)   	  (+  S02).
                                        89

-------
Whole Plants
     A final analysis of the hydroponically grown plant material involved
determination of sulfur content for shoots and roots.  Shoot and root sulfur
content did not vary significantly between the early and late season periods
in unfumigated plants (P ^ 0.05) (Figures 11.5 and 11.7) while the influence
of nutrient solution sulfur was significant.  Similarly, shoot and root
sulfur contents varied only with nutrient solution sulfur and not the S0£
fumigation during both periods of the growing season (Figures 11.6 and 11.8).
Linzon e~t at. (1979) found elevated sulfur levels in white birch foliage and
associated low level visible 862 injury with a mean S0£ concentration of 1.1
pphm during the growing season in southern Ontario.  Lack of difference
between unfumigated and fumigated plant material sulfur content in our study
may be attributable to the short exposure interval.  It is noteworthy, however,
that nutrient solution sulfur content had a significant effect (P < 0.05) on
shoot and root sulfur, albeit that effect was somewhat different in the early
and late season periods.  In addition, shoot sulfur content was greater than
root sulfur content during both periods of the growing season with the only
exception occurring on A in the "double sulfur" solution.  That sulfur content
of dried, inactive shoots and roots varied, particularly in the early season,
is not readily reconcilable.    Perhaps shoot sulfur content is always greater
        0.4
5  0-3

-------
      0.5r
  CO
      0.4
  <
  
-------
  CO
  O
  I-
  cc
  LJ
  O
  z
  O
  O
  IT
  CO
        Deposition
   No S            Complete S
NUTRIENT  SOLUTION  SULFUR
Double S
Figure 11.8.   Sulfur content in shoots  and roots  following  late season
               exposure (+ 862).   	  roots    	   shoots .
than root sulfur content with any additional sulfur  accumulation in SC>2
exposure simply due to deposition upon the dried shoots.   In general,  Figures
11.5 to 11.8 express the not unexpected accumulation of  sulfur in plants as
nutrient solution sulfur changes from near zero to  twice the optimal level.
Shoot and root sulfur content data are probably indicative of a response
rapid enough to suggest true biological trends.

     Although differences were not significant, shoot-root ratios calculated
for plants from the early exposure period suggested  an enhanced shoot growth
in fumigated versus unfumigated plants which is most pronounced with the "no
sulfur" nutrient solution treatments (Table 11.1).   Although the same trend
seems apparent in the late season data, root biomass was less among all  the
nutrient solution treatments on D.  Hence, the high  s/r may be less indicative
of enhanced shoot growth and more so of reduced root growth.

     It is apparent that important physiological changes may occur in response
to S02-  At no time have we observed visible injury  symptoms in western
wheatgrass.  Yet, the altered sulfur balance in the  plants suggests long-term
effects of, as yet, unknown proportions.

                                  CONCLUSIONS

     Sulfur contents in blade tips of western wheatgrass was greater than in
middle or basal segments of the blade.  While a secondary transport scheme
has been suggested to account for the movement of sulfate to blade tips  and
                                     92

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margins in the transpirational stream, it is conceivable that tips are simply
exposed for a longer period of time than the lower, younger portion of the
blade.

     The duration of the exposure periods (147 hours) appeared inadequate to
discern any sulfur distribution  trends among whole leaves y-:t, fumigated
leaves contained more sulfur than unfumigated leaves in the early season
trials.

     Sulfur dioxide treatments had no effect on shoot and root sulfur content
but the effect of nutrient solution was significant.   Shoot sulfur content was
greater than root sulfur content during both periods of the growing season with
the only exception occurring on  the unfumigated control in the "double sulfur"
solution.

     Trends suggest that shoot-root ratios were greater in the early season
on the plot fumigated with S02 but the trend late in the season suggested
reduced root growth rather than  increased shoot growth.  Further controlled
exposure studies are required to document consistent reductions in root
growth in the late season.

                                  REFERENCES

Detling, J. K., M. I. Dyer, and  D. T. Winn.  1979.  Net Photosynthesis, Root
     Respiration, and Regrowth of Bouteloua gTao-il'Ls Following Simulated
     Grazing.  Oecologia (Berl.), 41:127-134.

Esau, K.  1965.  Plant Anatomy.  John Wiley and Sons, Inc., New York.  767
     pp.

Garsed, S. G., and D. J. Read.   1977.  The Uptake and Metabolism of 35S02 in
     Plants of Differing Sensitivity to Sulphur Dioxide.  J. Environ. Pollut.,
     13:173-186.

Guderian, R.  197~7.  Air Pollution.  Springer-Verlag, Berlin.  127 pp.

Halbwachs, G.  1963.  Utersuchnunger liber gerichete aktive strHmungen and
     strofftransporte in blatt.  Flora, 153:333-357.

Hoagland, Dr. R., and D. I. Arnon.  1938.  University of California Agri-
     cultural Experimental Station Circular no. 347.

Jacobson, J. S., and A. C. Hill, eds.  1970.  Recognition of Air Pollution
     Injury to Vegetation:  A Pictorial Atlas. Air Pollut. Control Assoc.,
     Pittsburgh, Pennsylvania.

JSger, H. J.  1976.  S-Lokalisation in S02 begasten Fichtennadeln.  Eur. J.
     For. Pathol.,  6:25-29.

Langer, R. H. M.  1972.  How Grasses Grow.   Edward Arnold Publishers, London.
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Lalichli, A.   1972.   Translocation of Inorganic Solutes.  Ann. Rev. Plant
     Physiol., 23:197-218.

Lauenroth, W. K.,  C. J. Bleak, and J. L. Dodd.  1980.  Sulfur Accumulation
     in Western Wheatgrass Exposed to Three Controlled S02 Concentrations.
     In: Bioenvironmental Impact of a Coal^fired Power Plant. Fifth Interim
     Report, Colstrip, Montana. E. M. Preston and D. W. O'Guinn  (eds.)
     EPA-600/3-80-052. U.S. Environmental Protection Agency; Corvallis,
     Oregon, pp. 147-152.

Leopold, A.  C., and P. E. Kriedemann,  1975.  Plant Growth and Development.
     McGraw-Hill Book Company.

Linzon, S. M. , P-  J. Temple, and R. G. Pearson.  1979.  Sulfur Concentrations
     in Plant Foliage and Related Effects.  J. Air Pollut. Control Assoc.,
     29:520-525.

Malhotra, S. S., and D. Hocking.  1976.  Biochemical and Cytological Effects
     of Sulfur Dioxide on Plant Metabolism.  New Phytol., 76:227-237.

Metson, A. S.  1973.  Sulphur in Forage Crops; Plant Analysis as a Guide to
     the Sulfur Status of Forage Grasses and Legumes.  Tech. Bull. No. 20,
     The Sulphur Institute, Washington, D.C.  24 pp.

Munch, E.  1926.  Die Stoffbewegungen in der Pflanze {Translocation in
     plants].  Fischer, Jena.

Preston, E.  M., and T. L. Gullett.  1979.  Spatial Variations of Sulfur
     Dioxide Concentrations on ZAPS During the 1977 Field Season.  In:
     Bioenvironmental Impact of a Coal-fired Power Plant, Fourth Interim
     Report, Colstrip, Montana.  E. M. Preston and T. L. Gullett  (eds.)
     EPA-600/3-78-021. U.S. Environmental Protection Agency, Corvallis,
     Oregon, pp. 306-326.

Rennenberg,  H., Schmitz, and L. Bergmann.  1979.  Long-distance Transport of
     Sulfur in Niootiana tdbaown.  Planta., 147:57-62.

Salisbury, F. B.,  and C. W. Ross.  1978.  Plant Physiology.  Wadsworth Pub-
     lishing Company. Belmont, California.

Tingey, D. T., L.  Bard, and R. W. Field.  1978.  The Relative Sensitivity of
     Selected Plant Species to Several Pollutants Singly and in Combination.
     In: The Bioenvironmental Impact of a Coal-fired Power Plant, Third
     Interim Report, Colstrip, Montana.  E. M. Preston and R. A. Lewis  (eds.)
     EPA-600/3-78-021. U.S. Environmental Protection Agency, Corvallis,
     Oregon, pp. 519-522.

Williams, G. J., and P. R. Kemp.  1978.  Simultaneous Measurement of Leaf and
     Root Gas Exchange of Shortgrass Prairie  Species.  Bot. Gaz., 139:150-157.

Wolozin, H., and E. Landau.  1966.  Crop Damage from Sulphur Dioxide.  J. of
     Farm Economics, 394-405.

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Ziegler, I.  1975.  The Effect of S02 Pollution on Plant Metabolism.
     Residue Rev., 56:79-105.
                                      95

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                                  SECTION 12

               EFFECTS OF S02  EXPOSURE  WITH NITROGEN AND SULFUR
            FERTILIZATION ON THE GROWTH OF AGROPYRON SMITHII RYDB.

         D. G.  Milchunas,  W. K.  Lauenroth, J.  L.  Dodd,  and T. J.  McNary
                                  ABSTRACT

               Exposure of western wheatgrass  (Agropyron  smi-thii
          Rydb.)  to 3.0 pphm S02  during the growing  season
          resulted in increased leaf  areas,  while at 5.4  and 9.1
          pphm S02 leaf area declined to near  Control levels.
          Nitrogen fertilization  increased leaf  areas with
          increasing levels of S02 indicating  that N fertili-
          zation can ameliorate the effects of S02 pollution.
          S02 x N interactions also resulted in  a shift in
          phenological development.  Nitrogen  fertilized  plants
          exhibited an increased  rate of senescence  and time of
          senescence for 9.1 compared to 3.0 or  5.4  pphm  S02,
          but only a more rapid rate  of senescence compared to
          the Control.  Nitrogen  fertilization without S02 also
          resulted in a more rapid rate of senescence. Dif-
          ferentiating between rate and time of  senescence is
          necessary when examining the effects of any compound
          which can be both a fertilizer and a toxic substance.
          No S02 x SO^ interaction was observed.
                             INTRODUCTION

     Sulfur dioxide is the most widespread air pollutant that is capable of
causing severe injury and damage to vegetation (Saunders and Wood,  1973;
Stern, 1968).  Plants vary greatly in their response to S02 (Guderian and Van
Haut, 1970).  This variation is due to their genetic composition, to their
response to environmental factors, to their nutritional status,  and to the
time and concentration of exposure to S02 (Guderian, 1977) .  Sulfur dioxide
can result in the general disruption of photosynthesis, respiration and other
fundamental cellular processes and thereby cause reduction in plant growth
and yield (Ziegler, 1975).  On the other hand, sulfur is necessary for the
general metabolism of plants because it is a major component of  amino acids,
certain vitamins, glutothione, coenzyme A, and also functions in the activa-
tion of certain proteolytic enzymes, in the formation of glucoside oils, and
of certain disulfide linkages that have been associated with the structural


                                      96

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characteristics of protoplasm (Ziegler, 1975).  Because of the nutritional/
phytotoxic effects of sulfur and the differences in species response, contra-
dictory results can be found in the literature with respect to plant growth
and yield as affected by atmospheric S02, soil sulfate, and the interaction
between the two sulfur sources.

     Cowling and Lockyer (1978) demonstrated that exposure of sulfur-
deficient perennial ryegrass to S02 at low concentration (2 pphm)  can
correct sulfur deficiency.  Additionally, they found no adverse effects of
S02 on plants supplied with adequate sulfur through the soil.  In contrast to
this, Bell and Clough (1973) measured 50 percent  reduction in yield  of  S 23 peren-
nial ryegrass, at concentrations of 7.3 pphm S02.  Faller (1971)  reported
that 57.7 pphm S02 had a favorable effect on tobacco leaf development even
when sufficient sulfate (0,  40,  80  and  240 ppm) was  available from the  substrate.
They further concluded that S02 was equivalent to sulfate as a source of
sulfur for plant growth.  Thomas et al. (1943) found 8.5 pphm S02  less  effi-
cient than sulfate and yield of fumigated plots with various amounts of
sulfate (0, 0.8,  1.5,and  10  ppm)  to be the same as yield of non-fumigated
checks.  Katz (1949), Setterstrom et al.  (1938),  Booth et al. 0-976), Brisley
and Jones (1950), Brisley et al. (1959), Daines (1968), Thomas et  al. (1944)
reported that crop yields were not significantly reduced by S02 when visible
injury symptoms were absent.   Guderian and Stratmann (1962), Lockyer et al.
(1976), and Tingey et al. (1971) demonstrated a suppression of plant growth
by S02 with no visible leaf necrosis.  Lockyer et al.  (1976)  observed a
reduction in yield of perennial ryegrass grown without addition of sulfate at
low S02 concentration and a reduction in yield of plants grown in  15.4  pphm
SC>2 irrespective of the addition of sulfate to the soil.  Leone and Brennan
(1972) found S02 injury was more pronounced in plants grown at higher sulfate
levels.  Eaton et al. (1971) observed no reduction in growth of cotton  and
tomatoes exposed to S02 (7.7 pphm)  but a 37 and 54 percent growth  reduction,
respectively, upon the addition of sulfate salts.

     In plant and animal nutrition, sulfur metabolism is closely related to
that of nitrogen.  Sulfur and nitrogen are utilized in growth according to a
stoichiometric relation which closely agrees with the elementary composition
of protein, the principal consumer of these elements (Dijkshoorn et al.,
1960) .  Aulakh et al. (1976) and Pumphrey and Moore (1965) reported maximum
yield for alfalfa with a total N:total S ratio of 11:1.  Increased sulfate
application improved N uptake and enhanced protein production (Aulakh et al.3
1976).  Further, evidence is accumulating that certain sulfur-containing
enzymes perform a vital role in interconversion of nitrogenous compounds
(Rendig and McComb, 1959).  Medvedev (1957) has postulated that sulfhydryl
groups, through their effect on protein structure, regulate to some degree
the course of ontogenetic development.  Because roots apparently have the
ability to reduce sufficient sulfate to provide for their own needs but do
not translocate appreciable amounts of reduced sulfur to the shoots (Salesbury
and Ross, 1969), the increased supply of readily available sulfur  from  low
levels of S02 exposure may actually enhance protein production and plant
growth (Ziegler, 1975).

     High levels of S02 fumigation (59.2 pphm) have been shown to  reduce
protein synthesis (Godzik and Linskens, 1974).  Constantiniodou and Kozlowski


                                     97

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(1979) reported a significant reduction in protein and total nonstructural
carbohydrate when Ulmus americana seedlings were fumigated with high levels
of S02.  The reduction in protein was accompanied by increases in free amino
acids (Godzik and Linskens,  1974).  Steinberg et al. (1950) proposed that the
chlorosis commonly shown by plants subjected to nutritional stress is accom-
panied by an accumulation of free amino acids.

     There is a need for further investigation of plant response to S02 x
SO^ x N because  1) there are contradictory reports on S02 x SO^ interactions,
2) very little information is available on S02 x N interactions, and 3) there
is especially a lack of information in this regard for native rangeland
species grown under field conditions.  Under natural conditions, changes in
humidity, light intensity, temperature (Ziegler, 1975), dew, mist, and rain
(Garsed and Read, 1977; Malhotra and Hocking, 1976) can affect plant uptake
of 862.  This study investigated the effect of three levels of S02 fumigation
and sulfur, nitrogen and sulfur plus nitrogen fertilization on the growth of
western wheatgrass (Agropyron smith-Li, Rydb.) in a natural grassland ecosystem.

                         MATERIALS AND METHODS

     The study area was located on the divide between the Powder and Tongue
River drainage basins in Custer National Forest, Montana (45°15'N, 106°E) .   A
split plot design was used with S02 treatments as the main plots and fertilizer
treatments as the split plots.  The objectives of the S02 treatments were to
maintain 30-day median S02 concentrations of zero (Control), 2 (Low),  5
(Medium), and 10 pphm (High)  throughout  the April to October growing season.
Each 0.52-ha treatment plot was subdivided into two replicates.  Sulfur
dioxide was delivered to the treatment plots through a network of aluminum
pipes located approximately 0.75 m above the ground surface.  Concentrations
were monitored with a Meloy Laboratories (Model SA 160-2) sulfur analyzer
through teflon lines located .within the plant canopy.  Analysis of the 1978
monitoring data resulted in S02 growing season means of <1.0, 3.0, 5.4, and
9.1 pphm for the  Control, Low,  Medium and High treatments, respectively.
Geometric mean concentrations of S02 during daylight hours were one-third
less than the 24-hour day values reported above.

     Four 1 x 2 m contiguous fertilizer plots were located in each replicate
for each S02 treatment.  Fertilizer treatments were:  Control, nitrogen (150
kg nitrogen/ha as ammonium nitrate), sulfur (15 kg sulfur/ha as magnesium
sulfate), and nitrogen plus sulfur (150 kg nitrogen plus 15 kg sulfur/ha) .
The treatments were applied in solution on April 15, 1978.  The amount of
water used in application of the fertilizers (equivalent to 5 mm rainfall)
was also applied to the Control plots.  Soils on the study area were clas-
sified as Farland silty clay loams.  Soil N and SO^ levels for the A^ll
horizons from soil pits adjacent to the fumigated plots averaged 0.1 percent N
and 0.1 meq. 301+"  • 100 g"1 soil.

     Ten Agropyron smithii plants on each fertilizer treatment-replicate were
marked by placing a large metal washer over the plant (i,e.}, 20 plants
per fertilization treatment per S02 treatment).  Growth of each plant was
assessed by counting the number of leaves and measuring, to the nearest mm,
plant height, green and brown length of each leaf blade and the maximum width
                                      98

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of the green and brown portions.  Each leaf blade was assumed to be triangular
for leaf area calculations.  Live and dead leaf areas were calculated separately.
Decreases in the area of individual leaves between sample dates were assumed
to represent leaf material added to the litter.

     Analysis of variance was performed using a split-split plot design with
the following breakdown:  main plot-S02 level; split plot - a N x S two by
two factorial; split-split plot-sample date.  Replicates were viewed as a
randomized block due to positioning.  Tukey's Q values were utilized to com-
pute least significant ranges (LSR) and identify significant differences be-
tween means (Sokal and Rohlf, 1969).

                                     RESULTS

     Significant sample date x S02 (P = 0.055) and date x nitrogen (P =
0.001) interactions were observed for average plant height.  Significantly
greater plant height occurred on the High S02 treatment than on the Control
(Figure 12.1).  Plant heights for the Low and Medium S02 treatments were
greater than the Control but were significantly lower than the High S02
treatment at peak plant height (^ 5 July).  Plant height was greatly enhanced
by N fertilization (Figure 12.2) showing the greatest effect at peak height.
The timing of peak plant height was not changed by either S02 or fertilizers.
Significant post peak declines were evident with nitrogen fertilization.
                     350r
                     300
                     250
                    K
                     200
                    z  150
                      100
                      50
                              LSR
1
J.
2 , i i I
                        Apr
                             May
                                          July
                                                August   Sept
 Figure  12.1.   Plant height  for  S02  treatments  (-
•Control, 	Low,
                        Medium, 	 High) across  all  fertilization  treatments.
               Date  x  S02,  P =  .055.  Use LSR^  for significance range  of  S02
               treatments within date; LSRg for  across  date within  S02  treatment,
               and LSR18 for across  S02  treatment across  date.
                                      99

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                         z i
                       Apr    May    June    July    August   Sept
Figure 12.2.    Plant height with (-
-)  and without  (	)  nitrogen
               fertilization across S02 treatments.   Date x nitrogen, P = .001.
               Use LSR2 for significance range of treatments within date; LSRg
               for dates within treatment,  and LSR18 for across treatments
               across dates.
     Analysis of average number of leaves per plant showed significant date x
N (P = 0.001) and date x S02 (P = 0.001)  interactions.  The significant time
x N interaction was due to an intersection of values rather than any signi-
ficant within date effect of nitrogen fertilizer as indicated by LSR values.
The response to S02 was not clear but suggested a greater average number of
leaves per plant at the end of the growing season (Figure 12.3).

     Total leaf area (live and dead)  displayed a significant response to N,
S02, and sample date with the date x  N x  S02 three-way interaction signi-
ficant at P = 0.021.  Nitrogen fertilization increased total leaf area within
all S02 treatments and nearly doubled on the high S02 treatment at peak area
(Figure 12.4).   Post-peak leaf area differences progressively decreased with
time for S02 treatment with nitrogen compared to without nitrogen fertilizer.
Sulfur dioxide treatment without additional nitrogen did not generally show
significant differences in total standing leaf area although there was a trend
toward greater leaf areas with S02 treatment at peak and post peak dates.
Nitrogen fertilization resulted in substantial differences among S02 treat-
ments.  Leaf areas on the High S02 treatment were significantly greater than
Control on all except the first and the last two dates, and were also signi-
ficantly greater than those from the Low or Medium treatments up to the peak.
                                     100

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                      9r
                    LJ 4
                        April   May
                                          July
                                                August
                                                      Sept
Figure 12.3.
Average number of leaves per plant for S02 treatments.   (	
Control,	Low, 	 Medium,	High) Date x S02,  P =
.001.  Use LSR^ for significance range of S02 treatments within
date, and LSR9 for dates within S02 treatment.
Post peak leaf area on  the high S02 with nitrogen treatment declined more
rapidly than other treatments and reached levels similar to the Control on
the last sample date.

     Analysis of total  live leaf area illustrated S02 and nitrogen effects.
Date x S02 and date x N interactions were both significant (P = 0.001).  Live
leaf areas of plants on the Control plot were significantly lower than those
exposed to the high S02 concentration with the exception of the first sampling
date when the plants were very small (Figure 12.5),   Pre-peak increase was
greater and post-peak decline was more pronounced on the High S02 treatment
compared to Low or Medium treatments.  Nitrogen fertilization produced more
rapid pre-peak increases and post-peak declines in live leaf area (Figure 12.6)
Very large differences  between live leaf area with and without nitrogen became
insignificant by the September 15 sampling date.

     Total leaf area is a measure of the plant response as a whole.  Examin-
ation of individual live leaf area gives a more distinct picture of the
dynamics of growth because values for any given treatment/date combination do
not represent an average across all leaf age classes which would include
young expanding leaves  as well as old senescing leaves.  We will examine data
                                      101

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                                          /
                                            \
             April
August
                                                     Sept
Figure 12.4.
Total standing leaf area for S02 treatments (	 Control,
	Low,	Medium,	High)  with (•)  and without
(O) nitrogen fertilization.  Date x N x  S02, P = .021.  Use
LSR2 for significance range of N fertilization within S02 treat-
ment within date, LSR^ for across S02 within fertilization within
date, LSR8 for across S02 across fertilization within date, LSRg
for within S02 within fertilization across date, and LSR}8 for
across S02 across or within fertilization across date.
                                     102

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        800r
                                                               \
                                                                  \
                                                                    \
                                                                    \
             April
                    June
July
August
Sepi
Figure 12.5.
Total live leaf area for S02 treatments (	 Control, —	
—Low,	 Medium,	—- High) across all fertilization
treatments.  Date x S02, P = .001.  Use LSR^ for significance
range of SC>2 treatments within date, LSRg for within S02 treat-
ment across date, and LSR18 for across SC>2 treatment across date.
                                     103

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                                         July   August  Sept
12.6.    Total live leaf area with (-
                                                 -)  and without  (	)  ni-
               trogen  fertilization across all  S02  treatments.   Date  x  N,  P  -
               .001.  For  explanation  on use  of  significance  ranges  (LSR)  see
               Figure  12.2.
for leaf numbers four and five because their growth period and  our  sampling
dates coincide to  best  display  growth dynamics.

     The influence of nitrogen on live leaf area is demonstrated by the date
x N * S02 interaction (P = 0.001)  for leaf number 4 (Figure 12.7).   Two
aspects of this interaction will be discussed:   1) the influence of nitrogen
fertilization within S02 treatment, 2) the relationship between S02 treatments
without N fertilizer compared to the relationship between S02 treatments with
N fertilizer.

     Within S02 treatments,  nitrogen fertilization resulted in much larger
leaf four live area during early June compared  to the non-fertilized treat-
ments.  By the 26  June sample date, larger live leaf area with N fertilizer was
observed only on the Low and Medium S02 treatments.  Near the end of the
growing season, live leaf area-OIL the low S02 treatment was significantly
greater without nitrogen fertilization.

     Nitrogen fertilization altered the relationships among S02 treatments
for live area of leaf number four.   Early June  live leaf areas were not signi-
ficantly different in the absence of N fertilizer.  With N fertilizer,
significant differences were observed between S02 treatment.  A trend of
distinct ordered increase in live leaf area with increasing S02 level was
evident.  By late June, exposure to S02 significantly increased live leaf
area without nitrogen only on the Low  treatment.  With nitrogen fertiliza-
tion, significant increases in live leaf area were observed on the Low and
the Medium S02 treatment for June and July.  Live leaf areas on all S02

                                      104

-------
    E
    e
    LJ
    <
    LJ
        300 -
        250 -
        200
         150
         100
         50

               /A
              /'/^A
             April
        May
June
July
August
Sept
 Figure 12.7.
Live leaf area for leaf number four by  S0£  treatment (	
Control,	Low,	Medium,	High) with  (•) and
without (O)  nitrogen fertilization.  Date x N x  S02, P =  .001.
For explanation on use of significance ranges (LSR)  see
Figure 12.4.
treatments with nitrogen converged by the 16 August  sampling date.  Nitrogen
fertilizer induced a  rapid decline in live leaf area on  the high SC>2 treat-
ment with nitrogen which was not evident on the High S02  treatment without
nitrogen.

     Sulfate fertilization had only a small influence on  live leaf area as
demonstrated by the significant date x N x SO^  interaction (P = 0.036) for
leaf number five (Figure 12.8).  The interaction was significant largely because
                                    105

-------
                     300-
                        April    May
                                      June
                              July
August   Sept
Figure 12.8.
Live leaf area for leaf number five by nitrogen and sulfate fertili-
zation treatment across all S02 treatments.  Control  (	),
SCV (	) , N (	) , N + S04 (	) .  Date x N x
S04, P = .036.  Use LSR^ for significance range of fertilization
treatment within date, LSR9 for across date within treatment, and
LSR18 for across date across treatment.
of the convergence of data late in the growing season.  Significant inter-
actions involving SO^ were not observed for any other leaf area parameter
analysed.  Sulfate plus nitrogen fertilizer on the non-fumigated control
plants showed an increase compared to N alone but this was not statistically
apparent.  No sulfate x S02 interactions were observed.

     The amount of the total calculated leaf area which was transferred to
the litter during the growing season was significantly (P = 0.001) influenced
by the interaction of sample date, nitrogen additions, and S02 exposure
(Figure 12.9).  Significantly greater late season litter production was
observed for N compared to no N fertilization within S02 treatment and for
the High S02 treatment compared to other S02 treatments within N fertilization.

                              DISCUSSION

     The lack of a significant response to sulfate (without N) across S02
treatment is consistent with findings of Das and Runeckles (1975) , Lockyer  e~t
                                     106

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                       700 -
                         April    May
                                     June    July    August   Sept
Figure 12.9.
Litter area production for S02 treatments (	Control,
	Low, 	Medium,	High) with ( •) and
without (O) nitrogen fertilization.  Date x N x S02,  P =  .001.
For explanation on use of significance ranges (LSR) see
Figure  12.4.
al. (1976), Setterstrom et al.  (1938), and Thomas et al .  (1943) .  Faller
(1971) reported minor yield variations in tobacco plants  grown at 0, 40, and
80 ppm S0= and exposed to 57.7  pphm S02 but a slight yield depression with
the very high 240 ppm SO^ treatment.  Eaton et al .  (1971) reported 37 and 54
percent growth reduction in cotton and tomatoe, respectively, when 300 me/1
was supplemented to fumigations at 7.7 pphm S02.  Fumigating tobacco plants
with 201.5 pphm S02, Leone and  Brennan (1972) showed a positive growth response
when SO^ levels were increased  from a suboptimal 1.5 ppm  to 96 ppm SO^; and
then a depression in yield with 384 ppm
     Tobacco was used by both Faller (1971) and by Leone and Brennan (1972)
and their 240 ppm and 384 ppm SO^, respectively, applications were 3 and 4
times greater than the 80 ppm considered adequate for tobacco.  Comparison of
these studies to our SO^ treatment is difficult because of problems in con-
verting to ppm in field conditions.  However, if we assume that SO^ was con-
fined to a 10 cm soil depth, soil bulk density of 1.35, and soil water of 10
percent with all SOjf dissolved, our application of SO^ would be 665 ppm.  Regard-
less of the accuracy of the estimation, it is clear that SO^ application was
also very high.  High soil sulfate concentrations are not toxic to plants
because the tightly controlled mechanism for SO^ uptake by roots when adequate
levels are present in the plant prohibits indiscriminate uptake of additional
                                     107

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sulfur.  It is possible that high SO^ concentrations in the soil could in
some way interfere with metabolism of other essential nutrients and indirectly
affect plant growth.  Jordan and Reisenhauer (1957)  have suggested that S02
may interfere with calcium uptake.  Data from this study indicated no S02 x
S0= interaction under field conditions with very high SOZJ; application and
suggests that naturally occurring soil sulfur levels are not directly a
factor in plant susceptibility to S02.  These findings are in agreement with
Lockyer et al. (1976) who found that concentrations  of 0, 1.9, 3.8, 7.7 and
15.4 pphm S02 and 0 and 10 yg S0= kg"1 dry soil produced no soil treatment
effect.

     There have been documentations of an increase in the number of leaves
per plant with exposure to S02 (Ashenden and Mansfield, 1977; Bleasdale,
1973; Heitschmidt et al., 1978).  Our data showed a  significant increase in
the average numbers of leaves per plant only on the  Low S02 treatment.
Bleasdale (1973) suggested that exposure to S02 enhanced cell division by
interfering with the balance between oxidized and reduced sulfur radicals.
If this mechanism was causitive, one would expect an equal or greater re-
sponse with increasing S02 concentration.  Average number of leaves per plant
in this study parallel the response of individual live leaf area to S02 and
suggests a fertilization/toxicity controlled mechanism.  This is supported by
reports of reduction in the number of leaves with S02 exposure; i.e.,  Ashenden
(1978) 11.1 pphm in Daotyl'ls glomeTata, Ashenden (1979) 7.5 pphm in Poa
protens-is but not Daotyl-is glomeTata, Bell and Clough (1973) 13.2 pphm in
S23 ryegrass.

     The expected increased growth with N fertilization was observed in this
study.  What is interesting are comparisons of growth patterns with and
without N across date, S02 treatment;, and S02 treatment and date.  The live
leaf area of control plants with N was significantly greater at peak growth,
but this did not continue as the growing season progressed.  The live leaf
area of plants receiving nitrogen fertilizer displayed a more rapid post peak
decline and converged with the live leaf area of plants that were not fertilized
with N.  Further comparisons of S02 treatments with  N to those without N show
that post peak total leaf areas converged but remained higher and litter pro-
duction increased at greater rates with N fertilization as the season pro-
gressed.  Several important implications may be drawn from this.  First it
will be important to differentiate between and define rate of senescence and
time of senescence.  Rate of senescence is the increase in dead tissue, or
the decrease in live tissue, with time.  Time of senescence is the absolute
amount of live tissue remaining at a particular time.  In comparing between
two treatments then, rate of senescence may be greater even though time of
senscence is not.  This was the pattern observed in  plants fertilized with
nitrogen compared to plants not receiving nitrogen fertilizer.  Rate of
senescence can be a function of a fertilization effect rather than a toxic
effect and has no bearing on toxicity unless absolute live areas are also
reduced.  The large differences in treatments observed at the height of the
growing season with the eventual converging of data  as the growing season
progressed also indicates that final harvest data may underestimate treatment
effects when consumption occurs throughout the season as in a grazing rather
than a crop situation.
                                     108

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     Without N fertilization significantly increased plant growth was observed
only on the Low SC>2 treatment.  Live leaf areas for the Medium and High S02
treatments were neither significantly lower than the Low S02 nor significantly
higher than the Control.  This may be viewed as a peak S02 fertilization
effect at the Low concentration and approaching the point on the High S02
treatment where toxic effects begin to counteract the fertilization effect.

     With N fertilization a quite different response was observed between S02
treatments.   Nitrogen fertilization resulted in increased peak growth with in-
creasing level of S02.  Post^-peak growth was significantly greater on Low and
Medium S02 treatments with N, while only significantly greater on the_Low S02
treatment without N fertilization.  Our highest S02 concentration with N
fertilization displayed a time shift in leaf area distribution.  Total leaf
area was greater than all other treatments at pre-peak and peak growth periods
and then declined more rapidly.  Post peak live leaf area on the N plus High
S02 treatment was also significantly less than those found for the Low or
Medium S02 treatments.  Litter area within N fertilization was significantly
greater for the High S02 treatment.  These factors indicate a more rapid rate
of senescence and time of senescence for High S02 compared to Low or Medium
S02 with N fertilization, but only a more rapid rate of senescence compared
to the Control with N fertilization.  Because of the increased growth associ-
ated with S02 plus N fertilization, the observed senescence pattern may be
the result of a shift in phenology with earlier development and senescence,
as was observed with N fertilization alone, rather than a toxic effect which
would depress live leaf areas and growth.  Differentiating between rate and
time of senescence is necessary when examining the effects of any compound
which can be both a fertilizer and a toxic substance.

     Cotrufo and Berry (1970), Scurfield (1969), Zahn (1963), Enderlein and
KSstner (1967), Krauss (1967) and Materna and Kohout (1967)  have also observed
higher resistance to S02 in fertilized plants.  In Cotrufo and Berry's study,
0.5 g of NPK fertilizer per pot sharply decreased pine needle injury from
S02.  With 1 g of fertilizer per pot, even less injury was observed.   However,
when 2 g of fertilizer per pot was applied, tip necrosis was again evident.
Cotrufo and Berry could not explain a cause for the increased sensitivity to
S02 with high fertilizer applications but suggested there was an interaction
between high salt concentration of the needles and air pollution.  In this
study, N application was constant across three concentrations of S02.  We
also observed an ameliorating effect of nitrogen fertilization on S02 exposure
with an increased rate and time of senescence on the high S02 with N treatment.
These data indicate that the S02 x N interaction can be both positive and
negative and that the threshold between positive and negative can be altered
by varying either fertilizer or S02 concentrations.   Our data further indicate
that the assessment of positive or negative effects—of any one combination of
S02 and N is dependent on time.  A positive high S02 x N effect was observed
during the peak growth period while negative effects were observed during the
post-peak growth period.

     Studies on the effect of S02 on plant nitrogen metabolism suggest a
possible explanation for the increased rate of senescence on the High S02
plus N fertilized plants and the observation of Cotrufo and Berry (1970) .
Changes in free amino acid concentrations and enzymes involved in amino acid


                                      109

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metabolism have been found to be a typical response to S02 (Ja'ger, 1975;
Jager and Klein, 1977; Wellburn et al., 1976; Godzik and Linskens, 1974;
Malhotra and Sarkar, 1979).  Increases in free amino acid content at higher
S02 concentrations are probably brought about by protein hydrolysis (Malhotra
and Sarkar, 1979)-  Protein hydrolysis can eventually lead to tissue senescence
(Fischer, 1971).  Steinberg et al. (1950) proposed that the chlorosis commonly
shown by plants subjected to nutritional stress is the result of an accumula-
tion of free amino acids.  High NH3 levels are also observed in plants exposed
to S02 (Godzik and Linskens, 1974: Jager and Klein, 1977).  Both S02 and
ammonium nutrition increase the £P" ion concentration of cells and cause a
shift in the cation/anion ratio.  When the buffering capacity of the tissues
is exhausted, cell pH decreases.  Sulfur dioxide and N, while exhibiting a
synergistic fertilizer effect at low concentration, may in combination at
higher concentrations result in detrimental effects.

     The significant response to N fertilization within and between S02
treatments observed in this study demonstrates that N can ameliorate the
effects of S02 pollution by increasing the amount of sulfur plants can use
for growth and metabolism and thereby increase the atmospheric toxic concentra-
tion threshold.  However, negative effects may also result from nitrogen
fertilization with S02 exposure.  The balance between negative or positive
effects on plant growth is dependent on a complex interaction between soil
nitrogen level, S02 concentration, and time.  The validity of generalized
toxic concentration levels must be questioned when one considers that in
addition to soil nutrient status the effect of a given S02 concentration can
change in response to interactions of soil moisture, humidity, temperature,
wind, light, diurnal S02 fluctuation, synergism with other air pollutants, and
plant species composition.

     In a natural rangeland system the impact of fertilization or S02 pollution
must be assessed not only in terms of total productivity but also in view of
changes in the distribution of the resource in time and the quality of the
resource to consumers.  Forage quality of western wheatgrass from this study
area has previously been examined (Milchunas et al., -1980).  The distri-
bution in time effects observed in this study could have important implications
especially for non-domestic consumers.  A more rapid rate of senescence may
affect nutrient density by altering live to dead ratios and thereby affect
consumers.  Rumen bulk capacity and the rate of digesta breakdown and passage
through the alimentary tract can limit forage intake before the animals'
requirements for energy or nutrients are met (Milchunas et al., 1978).
Earlier senescence, irrespective of peak and mid-summer production, can
affect the length of time wild ruminants are subject to low quality forage.
This is a major factor in winter survival and spring natality rates.

                                 CONCLUSIONS

     No interaction of soil sulfate with S02 concentration was observed even
though SOit fertilizer applications were high.  Average number of leaves per
plant paralleled live leaf area responses to S02 and suggests a fertilization/
toxicity controlled mechanism rather than S02 enhanced cell division.   Sulfur
dioxide exposures significantly increased leaf area only on the low S02 treat-
ment.  Nitrogen fertilization can ameliorate the effects of S02 but can also

                                      110

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cause increased rate and time of senescence at higher S02 concentrations.   Ni-
trogen fertilization in the absence of S02 can result in a more rapid rate of
senescence.  Differentiating between  rate and time of senescence is  necessary
when examining the effects of any compound which can both be a fertilizer  and
a toxic substance.  Senescence can have an effect on consumers by altering the
seasonal resource distribution.

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Heitschmidt, R. K., W. K. Lauenroth,  and J. L. Dodd.  1978.   Effects of Con-
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                EFFECTS OF CHRONIC S02 EXPOSURE ON POPULATION
                           AND COMMUNITY STRUCTURE
                                  SECTION 13

                  SEED GERMINATION AND SEEDLING ESTABLISHMENT
                         AS AFFECTED BY SULFUR DIOXIDE

                       W. C. Leininger and J.  E. Taylor
                                   ABSTRACT

                 The effects of sulfur dioxide fumigation on range
            soils,  seed  germination,  and seedling  establishment
            were  studied  in  the  field  and  in the  greenhouse.
            Unpolluted soil  samples  were  seeded with seven peren-
            nial  indigenous  plant  species  and  exposed to  four
            levels  of   S02   fumigation   in   the   field.    Soils
            subjected to  five growing seasons  of  fumigation were
            seeded  similarly and  placed  in  an  unpolluted  green-
            house.  In  the field,    soil  sulfur  levels  after  8
            weeks  fumigation  increased  significantly with  rate.
            Green  needlegrass  (Stipa viridula )  exhibited  leaf
            necrosis  on  the  highest  sulfur  treatment.   Tissue
            sulfur  of   all   species  increased  with  fumigation
            intensity.   In  the  greenhouse,  the  soils from  the
            highest  sulfur  plot   (D)  had  6 times the sulfur
            content  of  the  control  (A) .   Germination  and  estab-
            lishment were  significantly  reduced  for five species.
            Nongraminoids were particularly affected.    Bluebunch
            wheatgrass (Agropyron  spioatwri)  and  green needlegrass
            accumulated  significantly  more sulfur  on D-plot than
            on  A-plot  soils.  Plant  height  and leaf  number were
            not  significantly affected  at any  fumigation  level.
            Volunteer  species were  more  abundant and  diverse  on
            the two lowest sulfur soils.
                                 INTRODUCTION

     Species  composition  of  plant communities affected by  chronic  air pollu-
tion  may  change   as  species  differentially  respond  to  the stress  factors
present.   Given adequate  time,  species may undergo  genetic adaptation.   More
immediate  symptoms could  be loss  of  sensitive  species  and/or  pathological
signs  in  others.   The  following changes  have  been  observed  in plants  in
response to  S02 stress  (ZAPS I and II):  increased leaf senescence in western
                                     115

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wheatgrass  (Dodd et al.,   1979a);  reduced plant  canopy coverage  and  species
diversity and species  composition  changes (Taylor and Leininger, 1979; Taylor
et al., 1980); and reduced reproductive viability (Rice et al., 1980).

     Species which do  not  show strong fluctuations in  population  density may
exhibit an  evolutionary  tendency  toward  lower sexual  reproduction (Stearns,
1977).  In many temperate rangeland plant species  this occurs, with vegetative
propagation assuming primary  significance in the  perpetuation and replacement
of most perennial species.   Nevertheless,  when disturbances occur which change
one  or more  of the habitat's  environmental variables  to levels  beyond the
tolerance or  competitive adaptability  of  some species,  sexual reproduction is
necessary for replacement  by  other species.   Also,  upon the subsequent relief
from  such disturbances,   former site  occupants which  have not survived the
stress period must re-enter the system by sexual means, if at all.  In such
situations, the  reproductive  performances of the component plant  species are
critical to the community's ability to adapt (Harper,  1965).

     Seed  development  and  dispersal and  seedling  establishment  are  complex
facets of sexual reproduction.   Rice et al.  (1980) looked at seed develop-
ment; we studied seed germination and seedling establishment under S02 stress.
The  study  occurred in  two  phases:   field observations  of  seedling establish-
ment  under  S02  fumigation  on soils which had not  been fumigated  previously,
and  greenhouse  observations of  seeds germinated in "clean" air in soils which
had been fumigated for five growing seasons.

      Lauenroth et al.  (1980) stated that sulfur concentrations within
plants were a function of growth rate,  duration of growing conditions, concen-
tration of  S02,  duration of exposure to  S02,  and  concentration of S02 in the
soil sulfur pool.  In order to isolate soil sulfur effects, we examined sulfur
accumulation  in the  tissues of bluebunch wheatgrass  (.Agvopyron spi-catiffn) and
green  needlegrass  (Stipa viridula  ), the  only two  of seven species producing
enough plant tissue for the analysis.
                             MATERIALS AND METHODS

Field Studies

     Samples of  soil  were  removed from the A-horizon (approximately top 7 cm)
of an area west of the ZAPS I site; slope, orientation,  elevation, and vegeta-
tion of  the  collection site were similar  to  ZAPS  I.   The collection site had
not been  subject  to  sulfur fumigation due to  distance  and direction from the
fumigation  site.   Soil was  placed  in perforated  metal  trays 34 x 50  x 9 cm
deep.  One  row of each of  seven  plant  species (Table 13.1)  was  planted at a
relatively  high  density   per  tray.   All seeds  were  from  indigenous  local
collections  on  nonfumigated sites.  Species  were selected  because  of their
economic importance and abundance in southeastern Montana.

     Seeding rates on a pure live seed (PLS)  basis were not calculated because
the purpose of the study was to observe establishment, sulfur accumulation and
pathologic signs  rather than percent germination.   It was  assumed  that since
both soils  and seeds  had  been taken from unpolluted sites,  seed germination
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TABLE 13.1.  NATIVE PERENNIAL PLANT  SPECIES  USED IN GERMINATION/ESTABLISHMENT
             STUDIES

Common Name
Western wheatgrass
Bluebunch wheatgrass
Sideoats grama
Green needlegrass
Wild flax
Purple prairieclover
Fourwing saltbush
Scientific Name
Agvopypon smithii
AgropyTori sp'Loatim
Bouteloua aurtipendula
Stipa vividula
Linum perenrie
Petalostemon purpureum
Atri-plex canes cens
Season of
Growth
Cool
Cool
Warm
Cool
Cool
Warm
Warm
Plant
Type
Grass
Grass
Grass
Grass
Forb
Forb
Shrub

should not be  affected by sulfur fumigation  in  the time period when the pans
were  exposed.   The species  were randomly  assigned to  rows  within each pan.
Four  replicated trays  were prepared  for  each  fumigation  treatment  and  an
additional tray was planted and taken to Bozeman to monitor plant development.
After  planting (22 May), each  tray  was  watered  to field  capacity  and  then a
set  of four replicates placed  on  each of the ZAPS treatment plots,  in loca-
tions  geometrically similar  to  the locations of gas  monitor C in each treat-
ment.

     Trays were watered during  the study to maintain good growing conditions.
On  20 June and  28 June  (29  and 37  days from  date  of planting)  trays  were
photographed and  examined for  seedling  number,  average seedling height,  and
average number of  leaves  for each species.   A record of leaf senescence also
was obtained on 28 June.

     On 25  July (64  days  after planting) trays  were  taken  to the laboratory
for analyses.   Average plant height and  average number  of leaves per species
were  calculated.   Average  length of  longest leaf  for  each  individual  was
determined and length  of  necrotic  tissue of the  longest  leaf measured.   All
plants  were  clipped  at   ground level  and  roots were  exhumed for  sulfur
analysis.

      Aboveground plant tissue was analyzed for sulfur using the procedures of
Tabatabai and  Bremner (1970)  as employed by  Hanson (1976);  soil samples were
analyzed with  techniques of Bardsley and Lancaster  (1960).  For no species was
there  sufficient root biomass for analysis.

Greenhouse Studies

     Soils were  collected  from  ZAPS I plots  A-D on 17 October 1979.  Collec-
tions  were  within 4  cm of  the soil  surface  (area of  greatest  natural seed
germination) and  at  the  same  distance from the gas  exit  pipes as monitoring
sensor C.  Soils were analyzed  for total  sulfur using techniques of Bardsley
and Lancaster  (1960).
                                      117

-------
     Hand sorted,  filled seeds of  western wheatgrass,  bluebunch wheatgrass,
and green needlegrass  (100  seeds  of each), and sideoats grama, purple prairie-
clover, wild  flax,  and  fourwing  saltbush  (50 seeds of  each)  were  planted in
randomized  rows  in  trays.   There  were four  replicate trays  per  treatment.
Trays  were  placed  under Sylvania  Grow-Lux lights, periodically  watered,  and
allowed 12  hours of  light  per day  to provide  favorable  growing conditions.

     Number of seedlings, average  number of leaves, and height of each species
were  recorded  every second or third  day  for  38 days  (through 3  March 1980).
Maximum germination was reached by day 17  for  six species;  western wheatgrass
reached maximum germination on day 25.  Plants were allowed to grow to accumu-
late enough tissue  biomass  to be analyzed.

    At the end of the experiment plants were harvested.  Bluebunch wheatgrass
and green needlegrass, grown in the A and  D treatment  soils,  were analyzed for
sulfur accumulations.

     During the experiment,  a striking difference in the numbers of volunteer
species (germinating from residual seeds in soil) was  noted.   After an addi-
tional three weeks  of growth, these plants were identified  to species and
counted in each tray;  species diversity (H')  (Shannon and  Weaver, 1949)  and
species richness (number of  species) were  calculated for each treatment.
                            RESULTS AND DISCUSSION

Field Studies

     The sulfur  content  of  the soils increased with fumigation (Figure 13.1).
This increase was  linear (P ^ 0.01) with exposure.  The fumigation rates used
in  the  correlations were monthly  averages  weighted by the number  of  days of
exposure in each month of the study.  Sulfur dioxide values were A = 1.23; B =
2.46; C  =  4.43;  and D = 6.85  pphm.   The soil from the A  plot had a signifi-
cantly higher sulfur  level  than the sample which had been removed to Bozeman,
suggesting contamination on  the ZAPS Control.  For this analysis, the Bozeman
site was assumed to be a sulfur-free environment, although no monitoring data
were available.  The  actual  site was approximately 6 km south of Bozeman in a
suburban setting with minimal sulfur sources nearby or upwind.

     The variation  associated  with sulfur measurements was quite  low  so that
statistically significant  step differences  were  detected between  ZAPS  A and
between levels.   The B and C exposure plots did not differ (P ^ 0.05).

     The phenomenon of  sulfur  accumulation in soils is well documented in the
literature  (Eaton  and Eaton,  1926;  Wilson,  1921).   Bertramun et ail.   (1949)
documented  absorption of atmospheric  sulfur by both  soils  and plants,  using
isotopic tracer techniques.   In the vicinity of a pollution source, the actual
amount  of  sulfur  absorption  by  soils  is  a  function of  distance  and soil
texture  (McCoal  and  Mehlich,   1938).   They noted  that  silty  soils  showed a
differential  sulfur  accumulation  with  distance  from pollution  sources, but
some clay  soils  did not.  In  our  study using silty clay  loam soils (Dodd et
al . , 1979b),  accumulation occurred over a very short time,  about  8 weeks.
                                     118

-------
                   40
                   30
                 E
                 Q.
                 Q.
                -520
                CO
                 o
                CO
                   10
                             0246
                         Bozeman ABC        D
                              S02  Levels (pphm)
                                              8
Figure 13.1.
Soil sulfur accumulated  on  ZAPS  I and Bozeman control after
64 days of fumigation (22 May  -  25 July, 1979).  Mean level
± 1 standard error is shown; *P  < 0.01.
     Plants  in the field were seriously damaged by rodent and rabbit depreda-
 tions  on  the  growing  seedlings.   Repeated  defoliation  reduced total  plant
 material  for  sulfur  analysis  and also  limited  our ability  to  take adequate
 measurements of leaf  numbers and lengths and plant numbers.

     Green  needlegrass  showed conspicuous leaf necrosis  (up  to  one-fourth  of
 the  leaf  length on D  treatment) with S02 exposure.  The damaged was  similar  to
 that described by Treshow (1970) and not observed on other species.

     The  accumulation of sulfur  in aboveground plant  tissue under S02 fumiga-
 tion is   shown in Figure 13.2.   Wild flax was not  analyzed because  it  lacked
 adequate  material.  Tissue sulfur levels in western wheatgrass were  similar  to
 those  reported by Dodd  et  al.   (1979a)  and  Rice  et at.  (1979).   Green needle-
 grass  values approximated  those  of Rice et al.  (1980).   These were the
 only species in  common  with  their studies  and ours.   Powers  (ND)  found that
 tissue sulfur  was higher in actively growing  plants.  The  similarity between
                                     119

-------
4800
4400
4000
3600
3200
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              ABCD   ABCD   ABCD   ABCD   ABCD
               Western     Bluebunch    Sideoats      Green       Purple
              wheatgrass   wheatgrass     grama    needlegrass   prairie clover
                                      S02 Treatment
                                                      ABCD
                                                       Fourwing
                                                       Saltbush
Figure 13.2.
Accumulation of sulfur  in
fumigation.
aboveground  plant tissue under SC>2
 our  observations  in  seedlings and  those compared  for mature  species suggest
 that  growth  stage  makes  little  difference  as  long as  plants  are  actively
 metabolizing.  There was  insufficient root biomass of any  species for chemical
 analysis.

      Plant  sulfur  correlations  are  presented  in  Table  13.  2.   All  species
 showed  positive  correlations  between  sulfur  fumigation  and  plant  sulfur
 content.
                                       120

-------
TABLE 13.2.
LINEAR REGRESSION AND CORRELATIONS  BETWEEN PLANT SULFUR AND  S02
FUMIGATION, ZAPS  I, 1979
Species
                  Regression Equation
Western wheatgrass
Bluebunch wheatgrass
Sideoats grama
Green needlegrass
Purple prairieclover
Fourwing saltbush
Y =
Y =
Y =
Y =
Y =
Y =
842.4+101.6 x
4.5 + 337.2 x
968.0 + 53.96 x
1501.9 + 56.3 x
1047.5 + 273.2 x
2525.0 +347.2 x
1 . 00*
0.98
0.88
0.89
0.94
0.85
1.00
0.95
0.77
0.80
0.88
0.72

    P  <  0.05.
     Although Treshow  (1970) pointed  out the  problem of  quantifying  atmos-
 pheric  sulfur levels  from plant  sulfur contents  and/or  the  degree  of plant
 injury,  our  data  suggest  that within  a local  vegetation type  and  climatic
 regime  such quantification may be  feasible.

 Greenhouse Studies

     There were  significant increases in sulfur among all treatments,  with the
 major  increase  between  treatments  C and  D  (Figure  13.3).  The  mean  sulfur
 level  for  treatment D was  more  than  six  times  the  level for  treatment  A.
3U
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                                Control  Low  Medium High
                                      Treatment
Figure 13.3.  Soil sulfur accumulation after five  growing  seasons  of  fumiga-
              tion.  Mean ± 1 standard error is  shown.
                                     121

-------
Differences  may have  indicated resistance  to  removal of sulfur  at  the lower
three  levels  of  fumigation  and/or  a  threshold  fumigation rate  (somewhere
between  C and  D)  against which plants  do  not effectively  remove sulfur.   It
also  could show the  secondary  effects  of  plant growth  inhibition  at higher
fumigation levels.   Because of  the reduced plant growth  and unthrifty plants
on D-plot, the  ability of  these plants to take-up and metabolize sulfur may be
reduced.

     We  intend  to  also determine  the pH, cation exchange capacity, electrical
conductivity,  and  organic matter  of  the  soils.   These  characteristics  have
important effects on  seed  germination.

     Western wheatgrass germination and  establishment  were similar at all
fumigation levels, although D-plot values were  consistently  higher (Figure
13 .4A).   Bluebunch wheatgrass  responded differently  (Figure 13.4B) in that
germination and growth occurred much quicker.   In this case, the soil with the
  100

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       A Low
       a Medium
       oHigh
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              D
        6  7
10   12
                         14
17   19  21     67
  Days after Seeding
10   12
                                                              14
                                                     17   19  21
Figure 13.4.   Number of live seedlings per 100 seeds; (A) western wheatgrass,
              (B) bluebunch wheatgrass, (C) sideoats grama, and  (D) green
              needlegrass.  Mean ± 1 standard error is shown.
                                      122

-------
highest level of sulfur enrichment depressed germination.  The warm season
grass, sideoats grama, showed similar patterns to bluebunch wheatgrass (Figure
13.4C), except that after day 12, seedling mortality increased at each sample
date.  By day 17, D-plot soil supported an average of 20 plants per 100 seeds,
while the A-plot had 70 plants.  Green needlegrass germination ceased at day
10 on the D-plot (Figure 13.4D).  Seedling loss at the higher sulfur rate was
less than observed with sideoats grama.  At the end of the study (day 19), the
High rate plot had one-half the plants of the Control:  33 vs. 66 per 100
seeds.

     The  germination  rate  was  significantly  lower  and  seedling mortality
higher for wild flax on the D-plot (Figure 13.5A). After day  10 there was a
linear decrease  in surviving plants,  and  at  day  17 the D-plot supported one-
tenth  the plant  numbers  of  the  other  treatments.   The  other  forb,  purple
 prairieclover, reacted similarly to flax  (Figure 13.5B), except that the C-plot
 (Medium sulfur exposure)  increased germination and survival  compared with all
other  plots.  Germination rate  was   significantly  depressed on  the D-plot.
Further,  this  treatment  showed a  reduction in  plant numbers  from  day  10
through  day  17-   On  the  D-plot the highest  germination  observed  was only 12
plants per 100 seeds.

     Fourwing  saltbush was  the  only shrub  studied  (Figure 13.5C), a species
characterized with a low germination rate  (Eddleman, 1978 and 1979).  Even so,
the  D-plot  germination and survival was  significantly  less  than  that  of the
other  treatments.   By  day 17,  survival  was  reduced to  three  plants per 100
seed, while  the  Control had 27  plants.

     From  these  species responses,  several generalizations can be drawn.  The
wheatgrass  did well  in both  germination  and survival  at  all sulfur levels.
For  all  other species, germination and survival were reduced on D-plot soils.
For  no species  did  any treatment except  D  significantly  lower  germination  or
survival  when  compared to  the  A  treatment.   In some  cases B  or C  plots
exceeded  A plots in plant  survival at the end of  the experiment, suggesting a
growth enhancement at lower levels of sulfur enrichment.  Forbs and the shrub
were more  adversely affected by S02-polluted  soils than grasses.

     There were  no significant  differences in number  of leaves  or heights of
seedlings  among  treatments.  It appears  that once seedlings  establish, growth
rate  is  not  affected  by  high  soil  sulfur levels and  other chemical changes
induced by fumigation.

     Plant tissue  sulfur levels for bluebunch wheatgrass and  green needlegrass
grown on  soils from plots  A and D are  shown in Figure 13 .6.   In both  species
significantly  higher  sulfur levels were  found in  the plants  from D-plot soils
compared to  those  on the A-plot.  This supports the idea that a portion of the
high  sulfur  tissue levels in  plants  found  in areas  of S02 fumigation comes
from the sulfur enriched soils.

     Species  composition  changes, which  still are  minimal,  have  appeared on
the  ZAPS  plots only during the past  two  years.   Therefore,  the residual seed
load  in  the  soil  should  not  differ   significantly  among  treatments.  Figure
13.7  illustrates differences in average  number of volunteer species (weeds)

                                     123

-------







•o
 ^ ^ ^ o "

67 10 12 14 17
                               Days after Seeding


Figure 13.5.   Number  of  live  seedlings per 100 seeds;  (A) wild flax,  (B)
              purple prairieclover, and (C) fourwing saltbush.   Mean ±
              1  standard error  is  shown.
                                    124

-------
                            2400
                          _ 2200

                          E
                          Q.
                          Q.

                          ~ 2000
                          3
                            1800
                            1600
                                   |  | Control
                                   k/V-1
                                   m
                                   Bluebunch
                                   wheatgrass
                               &
                                 Green
                               needlegrass
Figure  13.6.
Tissue  sulfur level for  bluebunch wheatgrass  and green needle-

grass grown on Control and High sulfur soils;  mean ± 1 standard

error.
140
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 Figure 13.7.
                   Control  Low  Medium High

                         Treatment


Number of volunteer species  (weeds)  per tray for four levels  of

fumigated soils;  mean ± 1 standard error.
                                        125

-------
per  tray at  the  end  of the  experiment for  the  four levels  of fumigation.
There is no significant difference in the number of species between the A-plot
and  the  B-plot  soils,  but both support  significantly more species than C and
D.

     The  volunteer plants  in  the  C  and D-plot  soils  germinated  much more
slowly  than those on  A-  and  B-plots.   Differences in  germination rates were
more striking in the  earlier phases of the study than at the time of  seedling
harvest.  According to Gordon (1972) seeds which  germinate slowly even under
favorable  conditions  are usually  the ones which will  not survive under more
typical  circumstances.  This  is because the favorable  period of plant growth
in  nature  usually is  short and  seedlings  which do not  become established
quickly die.

     The  diversity index  (HT) is  significantly higher for  volunteer plants in
the  B-plot  soils than for any other treatment  (Figure  13.8).   Values  for  the
D-plot are  significantly lower than values for A and  B.

     Species  richness  for volunteer plants follows a similar pattern  (Figure
 13  .9).   The  B-plot plants  are significantly  richer  floristically than the  C
and D treatments; D-plot had the fewest volunteer plants.
                                    SUMMARY

     Unpolluted soil placed on ZAPS I  for 8 weeks showed highly significant
linear increases in sulfur levels  with the SC>2 fumigation.   Soil on the A-plot
had significantly less  sulfur accumulation than on any of the other treatments.
The  D-plot  soil exceeded all others  (P  ^ 0.05).  Green needlegrass seedlings
exposed  to  S02  fumigation were necrotic  at  the high exposure rate.  Western
wheatgrass,  bluebunch wheatgrass,  sideoats grama,  green  needlegrass, purple
prairieclover  and fourwing  saltbush  all  showed  positive  linear increases in
plant  tissue levels with  increasing S02  fumigation.

      Soils  which have  been  fumigated  with S02  for five  growing seasons showed
significant  increases  in  sulfur  with  increasing pollution.   The D-plot  soils
had  more  than  6  times  as  much sulfur as  the control  soils.   Germination and
seedling  establishment were  significantly  reduced on the D-plot soils  for five
of the seven native species  examined.  This reduction was especially dramatic
for  the   forbs  and shrub.   Bluebunch  wheatgrass and. green  needlegrass showed
significant  increases  in  sulfur  when grown on  the  D-plot  compared to the A.
Growth,  represented by  plant height  and  number of  leaves, was not  signifi-
cantly affected  for  any species  by high  sulfur  levels   or  other  chemical
changes  in  the  soils  from  the High  fumigation plots.   For volunteer plants,
species  diversity, richness, and average  numbers were significantly less on
D-plot soils than  either  A or B.
                                  CONCLUSIONS

     The  sulfur  accumulation reported here probably occurred faster  than  that
 which  would happen  under  normal vegetational  cover  or  with  episodic  rather


                                      126

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-
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                                 Control  Low  Medium High
                                       Treatment
Figure  13.8.
Species diversity (H1) of volunteer  species (weeds) growing  in
fumigated  soils;  mean ± 1 standard error.
1 1_/
a
I 8
i Richness
species pe
CD
.3? "o 4
cjj 
-------
than continuous fumigation.  The  effects  which we observed may have consider-
able relevance in such  situations  as strip mine  revegetation  in the vicinity
of  coal-fired  power  plants or plant succession on stressed sites.   Also,  if
soils accumulate sulfur more readily than they lose it,  our  data may compare
with those from chronic  episodic  exposures.


                               ACKNOWLEDGEMENT

     The  authors  wish  to  express  their  appreciation  to  Dr.  Lee  Eddleman,
University of  Montana,  for providing the  seed for this study.   Also,  we are
indebted to Mr. Tim  McNary,  Colorado State University, for watching over the
field study in our absence.


                                  REFERENCES

Bardsley, C. E. and  J.  D.  Lancaster.  1960.  Determination of Sulfur in Soil.
     Soil Science  Society of  America Proceedings 24:265-268.

Bertramun, B.  R. , M.  Fried,  and  S.  L.  Tisdale.   1949.   Sulfur  Status  of
     Indiana Soils.   American Fertilizer 111(6):8.

Dodd, J.  L.,  W.  K.   Lauenroth,  G.  L.  Thor,  and  M.  B.   Coughenour.   1979a.
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     Corvallis, Oregon,   pp.  384-393.

Dodd,  J.  L.,  W.  K. Lauenroth,  R.  G.  Woodmansee,  G. L.  Thor,  and J.  D.
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Eaton  and  Eaton.    1926.   Sulfur  in Rainwater.   Plant   Physiology 1:77-87.

Eddleman, L. E.   1979.   Survey of Viability of Indigenous Grasses, Forbs, and
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Eddleman, L. E.   1978.   Survey of Viability of Indigenous Grasses,  Forbs and
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                                     128

-------
Hanson, D.   1976.  Procedure  for the Determination of Total  Sulfur in Plant
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Lauenroth, W. K. ,  C.  J. Bicak, and J. L. Dodd.  1980.  Sulfur Accumula-
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McCoal, M.  M.  and A.  Mehlech.  1938.  Soil  Characteristics  in Relation to
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Rice,  P.  M. , C.  C. Gordon,  and P. C.  Tourangeau.   1980.  Weight  and
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Stearns,  S.  C.    1977.   The  Evolution of Life Eistory Traits:   A Critique of
     the  Theory  and a  Review  of the Data.  Ann.  Rev. Ecol.  Syst.  8:145-171.

Tabatabai, M. A.  and J. M.  Bremner.   1970.   A Simple Turbulemetric Method of
     Determining Total Sulfur in Plant Materials 62:805-809.

Taylor, J. E., W. C. Leininger, and M. W. Hoard.  1980.  Plant Community
     Succession Studies  on ZAPS.   In:   The Bioenvironmental Impact  of a Coal-
     Fired Power Plant, Fifth Interim Report, Colstrip, Montana. E.  M. Preston
     and D. W. O'Guinn, eds.  EPA~60Q/3-80"052.  U. S. Environmental Protection
     Agency, Oregon. (In Press),  pp. 216-234.
                                     129

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Taylor, J. E. and W.  C.  Leininger.   1979.   Plant Community Changes  Due to Low
     Level S02  Exposures.   In:   The  Bioenvironmental  Impact of  a  Coal-Fired
     Power Plant, Fourth Interim Report,  Colstrip,  Montana.  E.  M. Preston and
     T. L.  Gullett,  eds.   EPA-600/3-79-044.   U.S.  Environmental  Protection
     Agency,  Corvallis, Oregon,  pp.  610-641.

Treshow,  M.   1970.   Environment and  Plant  Response.  McGraw-Hill, New York.
     422  pp.

Wilson, B.  D.   1921.   Sulfur Supplied to  the Soil in Rainwater.   J.  Amer.  Soc.
     Agron. 13:226-229.
                                    130

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                                   SECTION 14

      RESPONSE OF FIELD POPULATIONS OF SOIL NEMATODES AND ROTIFERS TO THREE
                 LEVELS OF SEASON-LONG SULFUR DIOXIDE EXPOSURE

        J. W. Leetham, T. J.  McNary, J. L. Dodd, and W. K. Lauenroth
                                    ABSTRACT

               Soil nematode and rotifer populations were sampled
          once in midseason in 1977 and 1978 in two field sites
          in southeastern Montana, an area included in the
          northern mixed-grass prairie region.  The two field
          sites were each divided into four 0.52 ha plots and
          fumigated with low-levels of S02 throughout the
          growing seasons of 1975-1979 (Site I) and 1976-
          1979 (Site II).  No significant treatment effects
          were found for the rotifers or three trophic groupings
          of the nematodes (herbivores, saprophages, and
          predators).  With the exception of predatory nematodes,
          significantly higher populations of all groups were
          found in the 0-10 cm soil layer than in the 10-20 cm
          layer.
                                  INTRODUCTION

     Soil nematodes and rotifers are ubiquitous in soils of  native grassland
ecosystems and are considered to have important roles in energy flow and nu-
trient cycling processes.  There is essentially no published information on
the effects of air pollutants and specifically S02 on the activities of  these
organisms.  There have been a few studies on the effects of  soil acidification
on enchytraeids and microarthropods  (Baath et al. ,  1980;  Abrahamsen et dl. 3
1978).  Artificial acidification caused reduced enchytraeid  populations  and
generally increased Collembola populations.  Soil mite (Acarina) populations
were unaffected by the changes in soil pH.  Sulfur dioxide has been shown to
be toxic to soil microorganisms involved in decomposition (Babich and Stotzky,
1974; Baath et al., 1980;  Abrahamsen et al. ,  1978;  Grant et al. , 1979;
Bryant et al., 1979).
                                     131

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                             MATERIALS AND METHODS

     Each of the treated plots within the two field sites was divided into
two equal replicates.   Both sites were sampled once in midseason in 1977 (14
July) and again in 1978 (24 July).   On each sampling date, five 5.0 cm
diameter by 20.0 cm deep soil cores were taken randomly on each replicate.
Samples were taken a minimum of 2 m from the delivery pipes.  In 1978 a fifth
treatment was created by sampling directly beneath the delivery orifices on
the High treatment plots.  The actual S02 concentration exposure at these
points was not measured but was considered to be at least double the concen-
tration away from the pipes.  The soil cores were divided into 10 cm increments
for extraction of nematodes and rotifers.  Extraction was by the Baermann
funnel technique.  All extracted material was preserved in a 1 percent  formalin
solution.  Taxonomic identification of the nematodes and rotifers was not
made, only a crude categorization was made based on the presence or absence
of stylets.  Stylet bearing types were considered largely herbivorous and
nonstylet  bearers  were considered largely saprophagous, although the stylet
bearers included some predatory and some fungal feeding nematodes.  The only
predator separated out was of the genus Mononehus.  Only total counts of
rotifers were made.

                                     RESULTS

     Nematode populations varied across sites and years (Figure 14.1).  Site I
had higher populations on all plots in 1978  while the population size on
Site II was about the same in both years.  Treatment effects were not apparent
and statistical tests were not performed on the total nematode population
estimates.

     A split plot ANOVA was performed on the 1978 nematode trophic group
(herbivores, saprophages, predators) data to test for treatment and depth
effects.  Since preliminary analysis indicated a linear relationship between
means and standard deviations for the saprophages, these data were transformed
[LN(X+1)J prior to the ANOVA.  For the other trophic groups analyses were
performed on untransformed data.  A significant treatment effect (P = .008)
was found only for the log transformed saprophagous nematodes on Site II
where there were significantly more saprobes on the High (7.5 pphm) treatment
than on the Control (Figure 14 .2).  All groups showed significant depth
differences.   For the herbivores and saprophages, there were significantly
higher densities in the 0-10 cm level than the 10-20 cm level (Table 14  .1).
There were higher densities of predators in the 10-20 cm layer.  The depth
distribution data for 1977 were essentially the same as in 1978 except an
even higher percentage  (over 90 percent)  of  the predators was in  the  10-
20 cm layer.
                                     132

-------
6

5
4
(0
2 3
i
9
DI977

-
-
-

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/










^tm
/
/








7"
/
'/
/





DI978




7
/
i^















      CO

      LJ
      CD
                          /
Figure 14.1.
   Control   Low   Medium  High    Orifice

     SULFUR   TREATMENT

Nematode densities in the top 20 cm of soil on two sites
in southeastern Montana.  A = Site I, B = Site II.
                                133

-------
          CO
          tr
          LJ
          QD
3.0
          +
          X
              2.5
              2.0
                   Control Low Med.     High
                       SULFUR  TREATMENT
                                          Orifice
Figure 14.2.   Season mean population densities of saprophagous nematodes
              on Site II on July  24, 1978 (vertical lines  are Tukey's Q
              value at x = 0.05).
TABLE 14.1.    VERTICAL DISTRIBUTION BY PERCENT OF SOIL NEMATODE POPULATIONS
              IN THE TOP 20 CM OF  SOIL ON TWO FIELD SITES  IN  SOUTHEASTERN
              MONTANA

Depth

0-10 cm
10-20 cm

0-10 cm
10-20 cm
Total

74.4
25.6

70.2
29.8
Herbivores Saprophages
Site I
71.5 83.1
28.5 16.9
Site II
64.4 77.2
35.6 22.8
Predators

12.0
88.0

43.2
56.8

     Stylet-bearing nematodes made  up a majority of the total nematode numbers
on both sites in both years (Figures  14.3 and 14.4).  A possible  treatment
response of  increasing herbivores and decreasing saprobes with increasing S02
exposure occurred on Site I in 1977, but was unsupported by either  the 1978
data or the  1977 and 1978 Site II data.
                                    134

-------

75


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P 25
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O
0 75
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UJ
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UJ
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0 Herbivores
. DSaprovores
/
/
P-

'
/
/
'
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_ b
~?
/
/
/
/
/
~
/
/
/
/
/
/
f
/
/
/
/
/
/
/
/
/
, /
^ /


/



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/

'
~| /

/
/
/

/
/
/
/
/
'
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7
/
/
/
/
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Figure 14.3.
                Control  Low  Medium  High  Orifice
                    SULFUR  TREATMENT
General nematode population  structure at Site I  by  percent
composition.   Predators were not included because they
were negligible by comparison.   A = 1977, B = 1978.
                              . a
                         CO
                         O
                         0_
                         5
                            75
                            50
                            25
                Q Herbivores
                D Soprovores
3 '5
j_
1 50
cr
LJ
O_
25
- D

.



7-
/
/
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;







_ j
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^
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_.
;/
7
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7
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Figure 14.4.
                 Control   Low  Medium  High   Orifice
                    SULFUR TREATMENT
General nematode population  structure at Site  II  by percent
composition.   Predators  not  included because they were
negligible  by comparison.  A =  1977, B = 1978,
                                        135

-------
     Rotifer populations were also variable across sites and years (Figure 14
   .5).   Densities were greater  on both sites in 1978  than in 1977 with Site I
300

250
200
150
100
10
O
X 50
evj
'E
- a

-
-
-
-
-







-

















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DI978




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              01
              UJ
              GO
     300


     250


     200


      150


      100


      50

Figure  14.5.
            Control Low  Medium  High Orifice


            SULFUR  TREATMENT

Rotifer densities in the top 20  cm of soil on two sites
in southeastern Montana.  A = Site I, B = Site II.
                                    136

-------
showing the greatest increase.  The site and year differences were not tested
statistically, however the 1978 data were tested with a split plot ANOVA for
treatment and depth differences.  No significant treatment differences were
found on either site, however, significant depth differences were found on
both sites (P<.01).  The average proportions of rotifer populations in the 0-
10 cm layer was 91 percent and 92 percent for Site I and II respectively.   The
figures for 1977 were essentially the same,  i.e.,  91 percent and 87 percent for
Site I and II respectively.

                                  DISCUSSION

     With the exception of the increased saprophagous nematode populations on
the high treatment of Site II in 1978", significant treatment responses were
not found in either nematodes nor rotifers.  This suggests that the S02
exposure of the field plots did not have any overall measurable effects on
either group.   However, since species identifications were not made,  it is
not known if any species may have responded to the exposure but their  popula-
tion changes were masked in the total counts.  The one case of significantly
higher saprophagous nematodes in the High treatment plot of Site II appears
not to be representative of any trend since none of the other data sets
support the finding.  It appears to be a chance occurrence, attributable to
the variability of the data.  If, indeed, the higher saprophagous densities
were due to SC>2 exposure, the reasoning behind such a shift might be that  the
nematodes increased in response to decreased microbial activity which  is
suspected from other studies (Leetham et al. ,  1980;  Dodd et al. „  1980).
The nematodes could conceivably be utilizing a resource left available by  the
decreased microbes.

     The higher nematode and rotifer densities near the soil surface are ex-
pected since the plant root biomass is similarly distributed (Lauenroth et
al., 1975).  The lack of significant treatment effects on the nematodes and
rotifers can be explained by either a lack of sensitivity or a lack of contact
with S02 or its derivatives.  The question of sensitivity to S02 cannot be
commented on since there is no published information on the effects of S02 on
either soil nematodes nor rotifers.  We suspect that the relatively low level
of S02 exposure to the soil surface did not result in any significant  chemical
changes below the surface because of the buffering capacity of the soil.
Leetham et al.  (1980)  have  shown that tardigrade  populations  in the upper 2
cm of the soil profile of these same plots were reduced by low-level S02
exposure.  For subsurface soil organisms, time may be the critical factor  in
whether or not chronic low-level S02 exposure will have an effect on their
population size and/or function.

                                  CONCLUSIONS

     No significant large scale changes occurred in field populations  of soil
nematodes and rotifers in the experimentally fumigated plots with the  possible
exception of an increase in nonstylet  bearing (largely saprophagous)  nematodes
on the high treatment plot of Site II in 1978.  However, the level of  identifi-
cation used in this study precluded the detection of responses in particular
species or genera.  Significantly higher populations of both nematodes and
rotifers occurred in the top 10 cm of the soil profile as compared to the 10-20

                                     137

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cm level.  The buffering capacity of the soil is thought to reduce or eliminate
the effects of S02 and/or its derivatives on the soil dwelling invertebrates
that occur below the surface 1. or 2 cm.

                                  REFERENCES

Abrahamsen, G., T. Hovland, and S. Hagvar.  1978.  Effects of Artificial Acid
     Rain and Liming on Soil Organisms and the Decomposition of Organic
     Matter.  SNSF-contribution FA 28/78.  23 pp.

Baath, E., B. Berg, U.  Lohm, B. Lundgren, H. Lundkvist, T. Rosswall, B.
     Soderstrbm, and A. Wiren.  1980.  Effects of Experimental Acidifi-
     cation and Liming on Soil Organisms and Decomposition in a Scots Pine
     Forest.  Pedobiologica.

Babich, H., and G. Stotzky.  1974.  Air Pollution and Microbial Ecology.
     Grit. Rev. Environ. Control,  4:353-421.

Bryant, R. D., E. A. Gordy and E.  J. Laishley.  1979.  Effect of Soil Acidifi-
     cation on the Soil Microflora.  Water, Air, and Soil Pollut., 11:437-
     445.

Dodd, J.  L. and W. K. Lauenroth.   1980.  Effects of Low-level S02 Fumiga-
     tion on Decomposition of Western Wheatgrass Litter in a Mixed-grass
     Prairie.   In: The  Bioenvironmental Impact of a Coal-fired Power Plant,
     Fifth Interim Report,  Colstrip, Montana.   E.  M.  Preston and D.  W.  O'Guinn
     (eds.) EPA-600/3-80-052, U.  S.  Environmental Protection Agency, Corvallis,
     Oregon.  (In Press) pp.  212-215.

Grant, I. F.,  K. Bancroft,  and M.  Alexander.  1979.   S02  and N02 Effects on
     Microbial Activity in an Acid Forest Soil.   Microbial Ecology,  5:85-89.

Lauenroth, W.  K., J. L. Dodd, R.  K.  Heitschmidt, and R. G.  Woodmansee.   1975.
     Biomass Dynamics and Primary  Production in Mixed Prairie Grasslands in
     Southeastern Montana:   Baseline Da.ta for Air Pollution Studies.  Fort
     Union Coal Field Symposium,  Eastern Montana College,  Billings,   pp. 559-
     578.

Leetham,  J. W., T. J. McNary, J.  L.  Dodd, and W. K.  Lauenroth.  1980.
     Response of Field  Populations of Tardigrada to Various Levels of Chronic
     Low-level Sulfur Dioxide Exposure.  Proceedings of VII International
     Colloquim of Soil  Zoology.

Lewis, R. A.,  A. S. Lefohn,  and N. R. Glass.  1976.   Introduction to the Col-
     strip, Montana, Coal-fired Power Plant Project.   In:  The Bioenvironmental
     Impact of a Coal-fired Power Plant,  Second Interim Report, Colstrip,
     Montana.   R. A. Lewis,  A. S.  Lefohn, and N. R.  Glass (eds.) EPA-600/3-
     76-013,  Environmental Protection Agency,  Corvallis,  Oregon.  pp. 1-12.
                                     138

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                                   SECTION 15

            ARTHROPOD POPULATION RESPONSES TO THREE LEVELS OF CHRONIC
           SULFUR DIOXIDE EXPOSURE IN A NORTHERN MIXED-GRASS ECOSYSTEM
                           I.  SOIL MICROARTHROPODS

         J. W. Leetham, J. L. Dodd, R. D. Deblinger, and W. K. Lauenroth
                                    ABSTRACT

               The effects of season-long exposure of soil micro-
          arthropods to controlled levels of S02 were investigated
          under field conditions from 1975 to 1978 in southeastern
          Montana.  Two field sites wherein three levels of S02
          were dispersed on 0.52 ha plots of grassland communities
          were used.  Periodic sampling was done throughout the
          growing seasons of 1975 and 1976 while only single,  mid-
          season samplings were made in 1977 and 1978.  Soil micro-
          arthropods were sampled by taking soil cores and extracting
          them in high-temperature gradient Tullgen extractors.
          Large scale population changes among the microarthropods,
          as a whole were not observed, however significant population
          reductions were observed for some groups.  The most
          notable reductions occurred in the Collembola where  three
          families (Poduridae, Entomobryidae-Isotomidae, and
          Sminthuridae) had significant population reductions  in
          the second year of S02 exposure on Site I.  Only a few
          acarine families showed significant population reductions.
          However, the affected groups included representatives of
          three main trophic or functional groups among the micro-
          arthropods - herbivores, fungivores,  and predators.   The
          data suggest that the greatest effects of S02 occurred
          during the first half of the growing season when soil
          water content and population levels were highest. The
          implications of the population reductions are discussed.
                                  INTRODUCTION

     Studies of the effects of air pollutants on soil microarthropods are very
few.  Most studies of pollutants and soil biota have dealt with microflora
and microfauna (bacteria, fungi, etc.).  Lebrun et at. (1977)  found a bark-
living oribatid mite, Humerobates Tostrolamellatus (Grandjean) very sensitive
to S02 exposure.  A concentration of 45 pphm (585 yg • m~3) for 48 hours

                                     139

-------
produced 50 percent mortality.   A followup study (Lebrun et al. ,  1978) found
that relative humidity had a substantial effect on the sensitivity of the
oribatid species to S02-   Mortality rates were significantly increased when the
relative humidity was increased from 20 percent to 80 percent while S02 con-
centration was held constant.  As will be noted later in this paper, the oribatid
mites compose a large portion of the soil microarthropod fauna on our field sites.

     Studies of artificial acidification of pine forest soils in Norway
(Abrahamsen et al., 1978) and Sweden (Baath et al., 1980) found increased
collembolan populations but only minor changes in the soil acarines.  Abraham-
sen et al., found two oribatid species were significantly reduced while
Baith et al. found  some oribatid population reductions, but none were signifi-
cant.  Both studies found populations of mesostigmatid mites were reduced
but not significant.  Also in both studies, the enchytraeid Cognettia
sphagnetorum (Vejd.) was  severely reduced in acidified plots.  The fact that
both studies were conducted in pine forest soils which are normally acidic
may account for the increased collembolan populations due to adaptation to
the acidic conditions.  These studies are relevant here since 862 can cause
acidification of soils, especially in the surface 1 to 2 cm layer where most
microarthropods reside.

                             MATERIALS AND METHODS

     Each of the treated  plots within the two field sites was divided into
two equal replicates from which random samples were taken.  All samples were
taken a minimum of  2 m from the delivery pipes (except for additional samples
taken beneath the pipes in 1977 and 1978).  Soil microarthropods were sampled
by taking 4.8 cm diameter by 5.0 cm deep  soil cores with  a coring tool designed
to minimize compaction and at the same time retain the sample in a 5 cm long
aluminum sleeve.  Vegetation cover was clipped to crown level prior to
sampling but surface litter was retained on the surface of the core.  A
Macfadyen-type high temperature gradient Tullgren extraction system was used
to retrieve the arthropods from the soil samples (Merchant and Crossley,
1970).  The extraction period was 7 days.  The arthropods were killed and  pre-
served in 70 percent ethyl alcohol and later counted and identified with a
binocular dissecting microscope.  Identification was to family and where
possible to genus,  but occasionally only to order.  Identifications below
family were hampered by the abundance of undescribed species, especially
among the Acarina.   For this study, "soil microarthropods" included the soil
acarines, apterygote insects, pauropods, symphylids and tardigrades.  Tardi-
grades are treated in detail in another paper (Leetham et at., 1979).
Representatives of various groups were dried at 60°C for 48 hours and weighed
for dry weight biomass.

     Site I was sampled  6  times  during the 1975 and 1976 seasons while
Site II was  sampled 6  times in the 1976 season.  Both sites were sampled
once in midseason in 1977 and Site I was sampled once in midseason in 1978.
Sampling intensity for 1975 and 1976 was five samples per replicate (10 per
treatment) per date.  Sample numbers were doubled in the  1977 and 1978
seasons (10/replicate).  Also in 1977 and 1978, an additional treatment
level was created by sampling directly beneath the delivery orifices on the
High treatment plot.  The S02 concentration at those points was not measured

                                     140

-------
but was considered to be at least double the concentration elsewhere on the
plot.

     A split-plot ANOVA was performed on the data to test for significant
treatment and date-within-year effects.  Because of the design of the field
experiment, we concluded that it would be illogical to include "sites" and
"years" as variables in the ANOVA.  Therefore, individual ANOVA's were
performed by group by year (or single dates in 1977 and 1978).  Since the
number of groups (orders and families) was quite large, ANOVA's were per-
formed only on those which displayed obvious trends in population changes
with increasing S02 fumigation (as judged by season mean density and/or
biomass in 1975 or 1976 or single samplings in 1977 and 1978).  Both density
and biomass were used in the ANOVA's.  It should be stated at this point
that although the traditional significance level of P =  0.05 was  used  as  a
guideline in judging population changes as significant, probabilities of 0.05
< P < 0.10 are also considered, primarily because of the inherently high
variability of the field data.  They were also used when similar population
changes occurred in more than one site-year for the same group.   In cases
where both treatment effects and date-by-treatment interactions were signifi-
cant, the interaction was given presidence over the main effect.   Tukey's Q
procedure was used to calculate least significant ranges to pinpoint where
the significant differences occurred.

                                     RESULTS

     The count to date of identified microarthropods includes 67  families of
Acarina,  six families of Collembola,  two families of Diplura  plus  tardigrades,
pauropods and symphylans.  A large majority of the soil microarthropod
community was composed of Acarina (Tables 15.1, 15.2, 15.3) with Collembola
being a distant second.  All other groups appear to be very minor.  Among
the Acarina the Prostigmata was by far the largest suborder with Cryptostigmata,
Mesostigmata, and Astigmata following in that order.  Large population
changes in response to S02 exposure are not readily apparent among most of
the major groups of microarthropods shown in Tables 15.1, 15.2,  and 15.3.

     Results of the statistical analyses are presented in Tables  15.4 and
 15.5,  All groups on which individual ANOVA's were performed are included
for comparison whether or not they had significant population changes.
Also, the results presented are for densities only since the results for
biomass were essentially the same.  Where differences occurred between
density and biomass, they will be discussed in text.

     First year fumigation effects among the microarthropods on ZAPS I are
evident (Table 15.4) but statistical support is lacking due primarily to
high variability of the data.   Of the groups that displayed trends of
reduced populations in the treated plots, only two were significant.  The
family Paratydeidae (Prostigmata) presented a peculiar response in that the
Low and Medium treatments were significantly reduced from the Control while
the High treatment was not (Figure 15.1A).   The same trend was found again
in 1976,  1977, and 1978 (Figures 15.1B,C,D).  Densities and biomass of
Oribatulidae (Cryptostigmata)  were reduced on all plots (Figure 15.2A).
Similar reductions occurred again in 1976,  1977, and 1978 but only those in

                                      141

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TABLE 15.1.   SOIL MICROARTHROPOD POPULATION STRUCTURE OF SITE I IN SOUTHEASTERN
              MONTANA*
       Group
                                               SC>2 Treatment
                                Density (Nos. • m~2)t
                           Control   Low
                                         Medium
                     High
                                Biomass (mg • m~2)
                    Control Low   Medium  High
       1975

       Total Microarthropods

       Acarina
       Suborders:
          Mesostigmata
          Prostigmata
          Cryptostigmata
          Astigmata

       Diplura

       Collembola
50,900  49,200  47,300   48,800   26.2

45,000  42,500  40,900   40,000   19.6
 1,800   1,500   1,500   2,300
34,100  34,600  32,700   29,600
 8,900   5,900   6,300   7,700
                 400
  200

  100

 4,300
  500

  100

4,300
  200

5,300
  400

  300

6,300
5.6
7.9
5.9
0.2

0.3

4.4
24.5

15.6

 2.3
 7.7
 5.2
 0.4

 1.0

 4.5
24.5

20.7

 7.9
 7.7
 4.8
 0.3

 1.6

 5.7
31.9

18.7

 4.4
 7.7
 6.3
 0.3

 2.8

 7.1
       1976
Total Microarthropods
Acarina
Suborders:
Mesostigmata
Prostigmata
Cryptostigmata
Astigmata
Diplura
Collembola
88,
70,

3,
55,
11,


15,
200
600

300
200
700
400
100
400
86,700
76,600

3,400
64,100
8,400
1,000
300
8,400
119,
106,

3,
88,
13,
1,

8,
200
600

100
700
700
100
400
300
89,
,, 79,

3,
67,
7,


6,
200
700

800
800
500
600
200
700
49.4
31.1

9.2
12.6
9.0
0.3
0.9
14.3
38.3
25.9

6.2
14.0
5.0
0.7
2.7
8.0
50.8
34.4

5.7
18.7
9.1
0.9
3.6
7.2
40.3
28.4

9.6
14.0
4.4
0.4
2.2
6.1
       * Figures are season means for the top 5 cm of the soil profile.

       t Numbers are rounded to nearest hundred.
 1978 were significant (Figure 15 .2C).   A significant date  by treatment
 interaction occurred in 1976 (Figure 15 .3B)  indicating the reductions were
 not significant on  the fourth sample  date.   Three date by  treatment  inter-
 actions were significant, one for the  suborder  Prostigmata and two for
 families Pyemotidae and Scutacaridae.   For  the  total Prostigmata, there were
 significantly reduced densities  in the High treatment plot on one sample
 date  (data not shown).  However,  the  same trend was not  evident on any  other
 date.   The two families, Pyemotidae and Scutacaridae, were quite similar in
 that  significant  treatment differences occurred only in  the spring and  early
 summer (Figure 15 .4) when they were most abundant on the field plots.
 During the remainder of the season their densities were  negligible.   In both
 cases,  densities  were significantly reduced in  the High  treatment plots.

       Collembolan  populations were significantly affected by S02 on Site I in
 1976  (Figures 15 .5  and 15 .6).  Total  collembolan density was reduced on all
                                          142

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TABLL 15.2.  SOIL MICROARTHROPOD POPULATION STRUCTURE AS MEASURED  IN MID-
             GROWING  SEASON IN 1977 AND 1978 ON SITE I*
                                          S02 Treatments
                           Density (Nos.  • m~2)t
Biomass (mg • m  )
Group
10 July 77
Total
Microarthropods
Acarina
Suborders:
Mesostigmata
Prostigmata
Cryptostigmata
Astigmata
Diplura
Collembola
8 July 78
Total
Microarthropods
Acarina
Suborders:
Mesostigmata
Prostigmata
Cryptostigmata
Astigmata
Diplura
Collembola
Control


84,800
82,600

2,500
71,100
8,000
1,000
<100
500


97,100
95,400

1,500
74,100
19,400
400
100
800
Low


111,000
108,900

3,500
90,700
12,300
2,400
0
300


69,400
68,300

2,200
53,400
12,500
200
<100
400
Medium


134,600
132,600

4,600
110,000
16,500
1,400
0
600


70,700
68,900

1,300
51,400
16,100
200
<100
900
High


65,000
64,200

3,500
52,300
82,000
200
0
200


72,700
71,300

2,300
57,900
10,600
400
100
500
Orifice


84,800
83,400

6,300
65,200
10,900
1,000
0
500


59,500
58,000

2,100
45,700
10,300
<100
100
900
Control


33.4
29.8

7.2
14.9
7.0
0.7
0.3
0.2


39.6
36.8

3.9
16.8
15.8
.3
.8
.8
Low


36.6
33.5

7.7
17.3
6.7
1.8
0.
0.1


27.5
26.0

5.7
9.9
10.2
.2
.5
.2
Medium


51.
49.

9.
24.
14.
1.
0.
0.


25.
23.

1.
10.
10.

•
•


8
5

7
4
3
1

1


3
2

9
9
3
1
3
7
High


29.0
27.8

8.3
11.8
7.6
0.1
0.
0.3


30.8
28.6

4.7
12.1
11.5
.3
.8
.3
Orifice


37.1
35.8

12.9
14.7
7.7
0.5
0.
0.3


21.9
19.7

4.1
9.1
6.5
<.l
1.3
.4

     * Figures are summaries for the top 5 cm of the soil profile.
     t Numbers are rounded to nearest hundred.
 treated plots, however, for biomass,  a  significant treatment-by-date inter-
 action resulted due to populations  on all  plots  being similar late in the
 growing season.  Treatment differences  occurred  during the first half of the
 season.  Within the Collembola, both  density  and biomass of Poduridae were
 significantly reduced on the treated  plots (only biomass data are presented
 in Figure 15.6).  Significant  treatment-by-date  interactions for density and
 biomass occurred for both the  Entomobryidae and  Sminthuridae. Members of the
 family Isotomidae were included in  the  Entomobryidae.  Since the entomobryids
 accounted for a majority of the total Collembola,  the similarity of Figures
  15.5B and 15.6B is expected.  There  were  reduced populations of Sminthuridae
 on all the treated plots on four of six sample dates (Figure 15.6C).

      Although density and/or biomass  reductions  occurred on one or more
 treated plots on Site I in many acarine groups after 1975, only a few of
                                       143

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TABLE 15.3.  SOIL MICROARTHROPOD POPULATION STRUCTURE OF SITE II IN SOUTH-
             EASTERN MONTANA*
                                         S02 Treatments
                            Numbers • m~2
Biomass (mg • m 2)
Group
Control
Low
Medium
High Orificet
Control
Low
Medium
High
Orifice
A-1976 Season Summary
Total
Microarthropods
Acarina
(Total)
Suborders:
Mesostlgmata
Prostigmata
Cryptostigmata
Astigmata
Diplura
Collembola
7 August 77 (One
Total
Microarthropods
Acarina
Suborders:
Mesostigraata
Prostigmata
Cryptostigmata
Astigmata
Diplura
Collembola

85,
71,


2,
58,
9,
1,

U,
Date)

63,
62,

3,
50,
7,




300
200


600
500
000
100
100
700


700
100

400
800
700
200
0
300

76,200
58,100


2,400
48,000
7,400
300
100
15,600


94,300
92,200

3,900
77,300
10,800
200
<100
600

130,100
94,600


3,000
77,200
13,400
1,000
200
12,000


143,300
121,000

6,100
100,300
14,400
200
<100
800

93,
76,


2,
62,
10,


12,


103,
99,

6,
79,
13,


700
700


700
600
600
800
200
400


500 49,200
700 46,900

600 2,100
400 39,700
000 5,000
700 100
<100 200
1,
700 1,500

42.8
28.9


5.8
12.6
9.7
0.8
1.2
10.0


24.8
22.7

4.0
11.6
6.9
.2
0
.3

41.1
22.4


6.4
10.1
5.6
0.3
0.9
14.7


37.1
34.2

5.1
17.1
11.9
.1
.3
.3

52.1
34.5


5.1
15.7
12.9
0.8
1.9
11.2


81.9
47.7

13.0
20.2
14.3
.2
.1
.7

47.4
27.8


4.1
13.3
9.8
0.6
1.5
11.5


47.2
41.8

10.1
18.3
12.8
.6
.5
1.5

-
_



-

-
-



17.7
14.0

2.4
8.0
3.5
.1
1.8
1.1
    *  Figures are for the top 5 cm of the soil profile.

    t  Sampled only in 1977 (see text).
those reductions were  significant.   Tectocepheidae (Cryptostigmata) density
and biomass were reduced on  the  treated plots in 1976 (density data are
presented in Figure 15.3).   The  little-known family Pediculochelidae (Pro-
stigmata) had significantly  reduced  densities and biomass in all treated
plots on 10 July 77 and a closely related but undescribed family (unknown
endeostigmatid, probably represented by just one species on the Sites) also
had reduced densities  and biomass on all treated plots on 10 July 1977.  Two
predatory families, Eupodidae and Rhagidiidae (both Prostigmata) had signi-
ficantly reduced densities and biomass  on all treated plots on 8 July 1978.
The plant-feeding spider mites,  Tetranychidae (Prostigmata), had reduced
densities and biomass  on all treated plots on 8  July 1978.  Density data for
the last five families mentioned are presented in Figure 15.7.
                                      144

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TABLE 15.4.   ANOVA RESULTS  FOR  SOIL MICROARTHROPOD DENSITIES  ON ZAPS I
                                    1975 Season          1976 Season     10 July 77   8 July 78
      Group                        Trt*    D x Tt       Trt     D x T        Trt        Trt


    Collembola                                          .062
       Entomobryidae                                    -       .067
       Poduridae                                        .016
       Ony chiur idae                  -}       -
       Sminthuridae                                     -       .006

    Protura
       Eosentomidae

    Symphyla                         -        -

    Acarina
       Astigmata
           Acaridae
       Prostigmata                   -       .003
           Alicorhagiidae             -        -                             -
           Anystidae                                    -        -         .016
           Bdellidae
           Cryp togna thidae
           Cunaxidae                                    -       .093
           Unknown Endostigmatid                   -                          .027
           Eriophyidae                                                                -
           Eupodidae                 -        -                                      .001
           Nanorchestidae                      -
           Paratydeidae               .058      -         .015      -         .009       .001
           Pediculochelidae                                       -         .066
           Pyemotidae                       <.001
           Raphignathidae
           Rhagidiidae                                                      -         .007
           Scutacaridae                       .004
           Tarsonemidae                                                      -
           Tenuipalpidae
           Tetranychidae                                                              .001
       Cryptostigmata                -
           Brachychthoniidae          -        -
           Ceratozetidae
           Gehypochthoniidae                             -        -
           Haplozetidae                                  -        -
           Inunatures (Total)
           Oppiidae                  -        -         -       .050
           Oribatulidae               .073      -         -       .006        -         .001
           Sphaerochthoniidae                            -        -
           Tectocephidae                                 .018


    *  Treatment main effect.
    t  Treatment by date interaction.
    t  Indicates the group showed a trend of season mean population reduction with S(>2 exposure,
    T  but reductions were not  significant at P < .10.  Blank spaces indicate no trends and  hence
       not tested statistically.
      Three  significant  treatment-by-date interactions occurred  for  the
 families Oppiidae  (Cryptostigmata),  Orioatulidae  (previously mentioned), and
 Cunaxidae (Prostigmata).   All three families  showed  consistent  trends  of
 reduced populations in  the  treated  plots with the greatest reductions  occur-
 ring in the  igh  treatment  (Figure  15.3).  A  significant  treatment  effect
 occurred for the  prostigmatid family Anystidae,  however the trend bore no

                                            145

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TABLE 15.5.  ANOVA RESULTS FOR SOIL MICROARTHROPOD DENSITIES ON ZAPS II
                                         1976 Season               7 Aug 77
  Group                             Trt*          D x Tt              Trt
Collembola
    Entomobryidae                      -t
    Sminthuridae                       -             .013

Pauropoda                              -              -

Acarina
    Astigmata
        Acaridae
        Hypopi
    Prostigmata
        Alicorhagiidae
        Unknown Endostigmatid                                           -
        Erythraeidae
        Eupodidae                      -             .003
        Nanorchestidae                .045            -                .001
        Nematalycidae                  -
        Pyemotidae
        Raphignathidae                 -
        Scutacaridae                   -             .063
        Tenuipalpidae                                                   -
        Trombldiidae                  . 040
    Cryptos tigmata
        Ceratozetidae                  -              -
        Immatures (Total)
        Galumnidae                     -              -
        Scutoverticidae               .047            -
        Tectocepheidae                                                  -
    Mesostigmata
        Laelapidae                     -             .017
*   Treatment main effect.
t   Treatment by date interaction.
±   Indicates the group showed a trend of season mean population reduction with
    S02 exposure, but reductions were not significant at P < .10.  Blank
    spaces indicate no trends and hence not tested statistically.
                                     146

-------
            770



            660



            550



            440



            330




            220-•



             no
         in

         I    0
         1
880




770




660




550




440




330




220




 110




  0
           3870


CED Control

    Low      3315

    Medium

CZD High

    Orifice   2760
            2210

            1660




             1105




             550
            2200




            1930




            1660




            1380



             1105




             830



            550




            275
                                                        \/

                                                        \/

                                                        \/

                                                        \/

                                                        \/

                                                        \/

                                                        \/

                                                        \/
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/

                                                                    \/
                                                                    \x
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/
                                                                    \/
                                      TREATMENTS
Figure 15.1.   Density estimates for  the  family Paratydeidae on ZAPS I.  A.

               1975 season means.  B.   1976  season means.   C.  10 July 77.

               D.  8 July 78.
                                      147

-------
         2100
         1800 -
         1500
        EI200
         900
        LU
        o
         600
          300
Figure 15,2.
Control Low  Med.  High   Control Low Med.  High   Control Low Med. High Orifice

                      TREATMENTS

 Density estimates of  two cryptostigmatid mite families on
 Site I.  A.  1975 season mean densities of the family
 Oribatulidae.  B.  1976 season mean densities of  the family
 Tectocepheidae.  C.   Densities of  the  family  Oribatulide on
 8 July 78.
relationship to SC"2 fumigation levels (data not shown).  There were  signifi-
cantly lower densities in the Low, Medium, and High treatments while the
Control and orifice densities were the same.  Since the actual numbers  of
individuals caught were low, we are not considering the significant  treatment
differences as reflecting S02 fumigation.

     Significant reductions in season mean densities on the  treated  plots  on
Site II occurred among two acarine families in 1976.   They were  the  fungivor^
ous Scutoverticidae (Cryptostigmata) and the predatory Trombidiidae  (Prostig-
mata).  The fungivorous family Nanorchestidae  (Prostigmata)  showed significant'
ly reduced densities on the treated plots on 10 August 1977.  However the
treatment differences in 1976 (data not shown) are quite different.   In that
year there was significantly greater densities and biomass in the Medium
treatment than the other treatments and Control which  were all  essentially
the same.  Data for these three families are shown in  Figure 15.8.  Signifi-
cant treatment-by-date interactions occurred among two acarine  families on
Site II in 1976.  They included the predatory  Eupodidae and  the  functionally
unknown Scutacaridae  (both Prostigmata).  In both cases, treatment differences
occurred early in the growing season at which  time densities were reduced  on
all treated plots, especially the High treatment plot  (Figure 15.9).  A
                                      148

-------
           in
           o
                                              2210"
                                              1660-
                                               1105-
                                               550-
                    MAR  MAY  JUN  JUL AUG  SEP
                                                     MAR MAY  JUN  JUL  AUG SEP
           CO
           2
                              2760-
                               2210-
                              1660-
                               1105-
                               550-
	 Control
	Low
	Medium
— - High
                                     MAR MAY  JUN  JUL  AUG SEP
                                         DATES  in 1976
Figure  15.3.    Time traces  of density estimates of three  acarine families on
                 ZAPS I in  1976.  A.   Oppiidae.   B.   Oribatulidae.   C.
                 Cunaxidae.
                                         149

-------
         16570-
         11050-
       v>
       o
       LU  5525-
                                	 Control

                                	Low

                                	Medium

                                	 High
                 APR MAY  JUN JUL AUG SEP
                                              22100-
                                              16570-
                                              11050-
                                              5525-
                                                     APR MAY  JUN  JUL AUG SEP
                                        DATES  in 1975
Figure 15.4.   Time  traces of density estimates of  two acarine familes on

                ZAPS  I in 1975.  A.   Pyemotidae.  B.   Scutacaridae.
   15







N~*
I

E


fO

2 10
 in
 o
 c
CO



LJ   5
        Control
 Figure 15.5.
                 Low    Medium


                  TREATMENTS
High
                                             40
                                         _  30
                                         
-------
in
t/i
O
CD
   2.5
   2.0
   1.5
   LO
  0.5
                            2.5 r
                            2.0
                             1.5
                             IX)
                            0.5
                                    	Control
                                    	Low
                                    	 Medium
                                    	High
                                                         1.0
                                                        0.8
                                                        0.6
                                                         0.4
                                                        0.2
      Control  Low  Medium  High

            TREATMENTS
              Mar May  Jun  Jul  Aug Sep      Mar May  Jun   Jul   Aug  Sep

                                   DATES in  1976
 Figure 15.6.
Biomass dynamics of  three  collembolan families on Site I in
1976.  A.  Season mean biomass  estimates of Poduridae.   B.
Time traces of biomass estimates  of  Entomobryidae - Iso-
tomidae. C.  Time traces of biomass  estimates of Sminthuridae,
 significant treatment-by-date interaction  occurred  for Sminthuridae (Figure
 15.10)  where the High treatment was significantly reduced from the Control
 on the  first sample date and the Low  treatment  on the third date.   The most
 notable aspect of the interaction  is  the consistently low densities on the
 High treatment throughout the season.  The significant interaction for the
 family  Laelapidae was erratic and  not considered to reflect any trends
 related to SC>2 fumigation.

      Many of the microarthropod groups included in  the ANOVA's had significant
 population changes across time.  Most of the  groups had seasonal trends like
 those depicted in Figures 15.5B, 15.6B, and 15.9A and B where the  populations
 were high in the first half of the season  and sharply declined during the
 second  half.  Because of the sharp population declines late in the season,
 treatment effects were not observable among many groups.  The S02  treatments
 appeared not to cause any major changes in the  timing of the late  season
 population declines.

                                    DISCUSSION

      Soil microarthropod populations  were  quite similar in size and structure
 on the  two field sites in 1976 when season mean populations are comparable.
 Although not tested statistically, there was  a  substantial difference between
 the 1975 and 1976 seasons on Site  I (Table 15.1).
                                       151

-------
            o
            c
            LJ
            O

125
100
75
50


?5


500

400
300
200
IUU




-


-

d


•

*










I — |






"5
h_
<§














3














2














.c
o>
i

400
300
200


100


5000

4000
3000
2000
1000

~|
0)
o
H-
6

-


•

f









— 1




3







"o
'c
o
o














J





"








2





h








i





| — |




—



«
o
600
500
400
300
200


100




^000
3000
2000
KX)O



-
-


•

f






















Control












1 -
r
Illl
                                       TREATMENTS
Figure 15.7.
Density estimates of five prostigmatid mite families on Site
I on 10 August 77 and 8 July 78.   A.   Pediculochelidae, 1977;
B and C.  The undescribed endeostigmatid family, 1977 and
1978 respectively;  D.  Eupodidae, 1978;  E.  Rhagidiidae,
1978; and  F.  Tetranychidae, 1978.
                                     152

-------

150
125
i
E 100

in
o
c
"7R
> 75
1-
co
z
Q 50

25









-

-












Control











O











•o
£











-C
en
X







300
200

100









i-

-












o
'c
o
O











-1











•a
a>











x:
Ol
X

6000
5000
*T\J \)\J



3000
2000

1000


-





















Control











3
o











T3

o
6
Figure 15.8.
                    TREATMENTS

Density estimates of three acarine families  on  Site II.   A.
Season mean  densities for Trombidiidae,  1976;   B.   Season
mean densities  for Scutoverticidae, 1976; and   C.   Densities
on 10 August 77 for Nanorchestidae.
              2000
                 ,_ a
                                  Control
                                            I5,000r
                                            10,000-
                                            5000 -
                 Mar  May   Jun   Jul   Aug  Sep      Mar  May   Jun   Jul   Amg  Sep
                                          DATES in 1976
Figure  15.9.    Time traces of density estimates for two prostigmatid mite
                families on Site  II  in 1976.   A.  Eupodidae and  B.   Scuta-
                caridae.
                                       153

-------
      4420
       3870
       3315
                         	Control
                         	Low
                         	Medium
                         	High
     fT
     '£
       2760
      in
      O
      LJ
      Q
       2210
        1660
            25 MAR
26 MAY    25 JUN    26 JUL   19 AUG

           DATES in 1976
                                                            19 SEP
Figure 15.10.  Time traces of density estimates for Sminthuridae  (Collembola)
               on ZAPS II in 1976.
     Three of the four family categories of Collembola had significantly  re-
duced populations on Site I in part or all of the 1976 season.  The  fourth
family, Onychiuridae, was not significantly affected by the S02 treatments
possibly because that group is more subsurface in hafritv- The  three  affected
families, Poduridae, Entomobryidae (including Isotomidae) and  Sminthuridae,
are all generally surface or near surface dwelling  (Leetham, unpublished
data from a shortgrass prairie).  Since 1975 was the first year of treatment
(beginning in June), 862 treatment may not have had sufficient time  to
affect the collembolan populations.  This argument  seems to hold  true for
Site II in 1976 where only the Sminthuridae were affected by S02  enough to
                                      154

-------
show population reductions.  In 1977 and 1978, the single samplings may have
been made after the critical moist part of the season when it appears the
S02 may have its greatest impact.  The 1976 date by treatment interactions
for the Entomobryiidae and Sminthuridae support this suggestion.  Seasonal
dynamics of most all the microarthropod groups follow closely the seasonal
soil water dynamics - i.e, , wet in spring and early summer, drying out in
late summer and fall prior to rewetting by fall and winter storms (Dodd et
al., 1979).

     Although trends of population declines among the soil acarines were
numerous, most were not statistically significant because of high sample
variability.  Where acarine population declines were significant, most
occurred during the first half of the season much as among the Collembola.
The inconsistencies of apparent population changes among the acarine groups
across years and sites adds difficulty in drawing conclusions about the
effects of S02 fumigation.  However, because there are so many trends, we
are concluding that S02 did have deleterious effects on the soil micro-
arthropods.

     The results of this study are not conclusive enough to support a statement
of differential sensitivity of the three major trophic classifications used
in this study - herbivores, fungivores, and predators.   Significant population
reductions occurred in representatives of all three.  Population changes
observed in this study are likely due to direct toxicity of S02 or its
derivaties on the microarthropods themselves, or a reduction in their food
resources through toxicity to prey organisms.  Reductions in fungivores is
probably due to reductions in food resources since there is ample evidence
that S02 and its derivatives have significant effects on soil microbial
activity (Babich and Stotzky, 1974) which probably reflects reduced microbial
populations.

     The ecological implications of microarthropod population reductions
from S02 or other anthropogenic contaminants are largely speculative primarily
because the functional importance of these organisms in ecosystem processes
is poorly understood.  In terms of energy flow as a function of density,
biomass, and respiration, the microarthropods are greatly outranked in the
soil by microbes and nematodes.  However, the importance of the microarthropods
may be more along the lines of how they influence the functioning of other
groups.  For example, the cryptostigmatid mites, which are largely fungivores,
can greatly enhance the activities of bacteria and fungi by distributing
inoculum (spores, etc.) among organic debris (Wallwork, 1970).  Parkinson et
at. (1979) suggest that fungal grazing by Collembola not only can spread
fungal spores, but may very likely alter competitive relationships of fungal
species complexes in litter and/or soil.   This same concept can be projected
to nematode-feeding microarthropods.

     If direct toxicity of S02 is the reason for a decline in the population
of one or more microarthropod species, then those same organisms may function
in the future as sensitive indicators of changes in the soil-litter system
as a result of exposure to anthropogenic S02.  The full impact of any changes
in the litter-soil system as a result of S02 exposure can only be evaluated
with time so that the long-term effects of small changes such as observed in

                                     155

-------
this study can be related to long-term alterations in ecosystem structure
and/or function.  Such was not the scope of this study.

                                 CONCLUSIONS

     Long-term, low-level S02 exposure resulted in significant population re-
ductions among a few of the soil microarthropod groups on the two field
sites, although their reductions were not large enough to affect the total
microarthropod population estimates or estimates of the dominant group, Acarina.
The acarines  accounted for over  90  percent of the microarthropods density and 70
percent of the biomass.  The most notable treatment effects occurred in
the apterygote insect order Collembola where significant population reductions
occurred in S02 treated plots for season mean collembolan density and the
season mean density and biomass of three family groups Poduridae, Entomo-
bryidae (including Isotomidae)  and Sminthuridae.  These reductions occurred
in 1976 on Site I, the second season of S02 fumigation.  No significant
population changes were observed in the first year of fumigation on either
Site I or II with the exception of Sminthuridae on some sample dates on Site
II in 1976.

     Among the Acarina, 11 families were observed to have significantly re-
duced populations on at least one site during the study.  Although the popu-
lation reductions were statistically significant on only one site-year
and/or time-date within a year,  trends for these same families and others
were observed at  other times or dates in the study.  High sample variability
was the principal reason for failure of many groups to show statistically
significant treatment effects.

     Sulfur dioxide effects were not restricted to one functional or trophic
group.  Among those families which had population reductions were representa-
tives of three important trophic groups, •i.e., herbivores, predators, and
fungivores.  Most population reductions observed in this study occurred in
the first half of the growing season when soil water conditions were highest.
This suggests that the effects  of S02 on microarthropods are magnified by
increased soil moisture, although the mechanism by which S02 caused the
population changes was not determined.  It is possible that both direct
toxicity and toxicity to food resources could have been involved in the
population changes observed.

                                   REFERENCES

Abrahamsen, G., J. Hovland, and S.  Hagvar.  1978.  Effects of Artificial
     Acid Rain and Liming on Soil Organisms and the Decomposition of Organic
     Matter.   SNSF-contribution FA 28/78.  23 pp.

Baith, E., B. Berg, U. Lohm, B.  Lundgren, H. Lundkvist, T. Rosswall, B.
     SOderstrom, and A. Wiren.   1980.  Effects of Experimental Acidification
     and Liming on Soil Organisms and Decomposition in a Scots Pine Forest.
     Pedobiologia.  (In Press)

Babich, H. and G. Stotzky.  1974.  Air Pollution and Microbial Ecology.
     Grit. Rev. Environ. Control, 4:353-421.

                                      156

-------
Dodd, J. L., J. W. Leetham, T. J. McNary, W. K. Lauenroth, and G. L. Thor.
     1979.  Baseline Characteristics of Producer and Invertebrate Populations
     and Certain Abiotic Parameters in the Colstrip Vicinity, pp. 53-106.
     In:  E. M. Preston and T. L. Gullett (eds.) The Bioenvironmental Impact
     of a Coal-fired Power Plant, Fourth Interim Report. EPA-600/3-79-044.
     U. S. Environmental Protection Agency.   Corvallis,  Oregon.

Lebrun,  P., G. Wauthy,  C. Leblanc, and M.  Goossens.   1977.   Ecologic Test
     of the Tolerance to SC>2 Toxicity in the Oribatid Mite EwneTobates
     Tostrolcmel'latus (Grandjean, 1936) (Acari: Oribatei).  Annales Soc. R.,
     Zool., Belg., 106:193.

Lebrun,  P., J. M. Jacques, M. Goossens and G. Wauthy.  1978.  The Effect  of
     Interaction Between the Concentration of S02 and the Relative Humidity
     of Air on the Survival of the Bark-living Bioindicator Mite Ewnevobates
     rostrolamellatus.  Water, Air, and Soil Pollut.,  10:269-275.

Leetham, J. W., T. J. McNary, J. L. Dodd, and W. K. Lauenroth.  1979.
     Response of Field Populations of Tardigrada to Various Levels of Chronic,
     Low-level Sulfur Dioxide Exposure.  Proceedings of VII International
     Colloquim of Soil Zoology.

Merchant, V. A. and D. A. Crossley.  1970.  An Inexpensive High Efficiency
     Tullgren Extractor for Soil Microarthropods.  J.  Ga. Entomol. Soc.,
     5:83-87.

Parkinson, D., S. Visser, and J. B. Whittaker.  1979.   Effects of Collembolan
     Grazing on Fungal Colonization of Leaf Litter.  Soil Biol.  Biochem.,
     11:529-535.

Wallwork, J. A.  1970.  Ecology of soil animals.  McGraw-Hill Publishing
     Company Limited, Maidenhead, Berkshire, England.   283 pp.
                                     157

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                          SECTION 16

   ARTHROPOD POPULATION RESPONSES TO THREE LEVELS OF CHRONIC
  SULFUR DIOXIDE EXPOSURE IN A NORTHERN MIXED-GRASS ECOSYSTEM
                   II ABOVEGROUND ARTHROPODS

J. W. Leetham, J. L.  Dodd,  R. D.  Deblinger, and W. K. Lauenroth
                           ABSTRACT

        The effects of continuous,  season-long exposure
   of aboveground arthropods to various levels of S02
   were investigated under field conditions in 1975 and
   1976 in southeastern Montana.  Three field plots
   (0.52 ha each) on each of two grassland community
   sites were  fumigated with S02 on the ZAPS  sites
   (Section 1).   Similar  sized  Control plots  were  in-
   cluded  in each  site.   Periodic  samplings were made
   throughout  the  1975  and  1976 growing seasons.  Above-
   ground  arthropods were sampled  by dropping a 0.5 m
   circular cage  over predetermined (but randomly
   chosen) sample  locations and retrieving the arthro-
   pods by vacuum.  Berlese funnel extraction and
   hand sorting were used to separate arthropods
   from debris.   Biomass  and/or density reductions
   occurred in a number of  insect  and acarine groups
   on  one  or both  sites.  The groups included Acarina,
   Diplura, Collembola  (Poduridae), Hemiptera
   (Pentatomidae), Homoptera (Cicadellidae),  Thysanoptera
   (Thripidae), Coleoptera (total)  Staphylinidae and
   Curculionidae, Diptera (Muscidae and Ceratopogonidae).
   These taxonomic groups were considered to represent two
   possible classifications of organisms showing popu-
   lation reductions.  One group included arthropods which
   were relatively immobile and strongly associated with
   the soil surface litter.  A second group included
   more mobile, flying  insects.  It is suggested that
   reductions in populations in the former group most
   likely involve toxic effects of S0£ or its derivatives
   directly to the organisms or their food resources.
   The mobility of the  latter group introduces the
   possibility of behavioral avoidance of the relatively
   small experimental plots.  Evidence to support these
   hypotheses is given.
                               158

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                                  INTRODUCTION

     The origin and importance of this study as a portion of a large, interdis-
ciplinary research project concerned with coal-fired power plant emissions on
northern mixed-grass prairie were discussed in Leetham e~k at. (submitted b).
This paper will concern responses of aboveground arthropods to long-term, low-
level sulfur dioxide exposure under field conditions.

     Three aspects of this study make it unique among studies of air pollutants
and arthropods:  1)  a system level orientation to responses of arthropods in
a native prairie to exposure to a major component of coal-fired plant emissions;
2)  the study area was considered pristine (i.e., no previous history of air
pollution exposure) prior to experimental fumigation with S02; and 3)  the
study was conducted under field conditions.  Of the few published studies
concerning insects and air pollutants, most are either a postenoi"i, in that
they were conducted sometime after the experimental areas were exposed to
pollution, or the studies were conducted under highly controlled laboratory
conditions.  For example, Freitag et al. (1973) studied carabid beetle
populations near a Kraft mill in Thunder Bay, Ontario, some years after the
mill had been operating, and found lower beetle populations near the mill as
compared to farther downwind.  Hillman and Benton (1972) concluded that S02
exposure from a coal-fired power plant in central Pennsylvania was responsi-
ble for reduced populations of social bees and parasitic wasps,  and the
reduced wasp population was, in turn, responsible for increased aphid popula-
tions.  They followed-up the field study by fumigating honey bee colonies
with S02 at various controlled levels between 0 and 500 pphm and found an
inverse relationship of brood-rearing and pollen collection with S02 con-
centration.  Ginevan and Lane (1978), using Drosoph-ila melanogaster and
controlled laboratory conditions found long-term, low-level S02 exposure (70
and 40 pphm) caused significant increases in developmental time and decreases
in survival.

                             MATERIALS AND METHODS

     The study area in southeastern Montana and design of the field experi-
mental plots were described in Leetham et al. (submitted b).  Aboveground ar-
thropods were sampled on  Site I   6  times in each 1975 and 1976 growing season
while Site II was  sampled 6  times  in the 1976 season only.  Samplings for a
given year were spaced at approximately  3 week intervals throughout the
growing season (April - September).

     For this study, "aboveground arthropods" were defined as those arthropods
occurring in or above the soil litter and aerial vegetation.  The arthropods
were sampled by dropping a circular cage over predetermined, but randomly
chosen, sample locations and vacuuming out the contents, including litter and
vegetation.  The cage covered 0.5 m2 and was dropped from a cart-mounted 18
foot (5.5 m) boom.  Cage contents were vacuumed in two stages:  1) a light
vacuuming of cage walls and aerial vegetation for active arthropods, and 2)
clipping and bagging of all vegetation followed by hand vacuuming to retrieve
remaining litter and plant refuse.  The first stage material was frozen then
hand sorted for arthropods while the second stage was subjected to Berlese
funnel extraction to retrieve the arthropods.  The two stage process was

                                      159

-------
found to have better efficiency of retrieval than other techniques such as
hand sorting and mechanical flotation.  All the arthropods were preserved in
70 percent ethanol and later counted and identified.  Five samples per repli-
cate  (10 per treatment) were taken on all dates, the sample locations being
chosen by use of a random numbers table.  Specific details of the collecting
and extracting equipment are given by Leetham  (1975).

     The arthropods were identified as far as possible which often was only
to family.  When possible,  voucher specimens were sent to recognized special-
ists for verification.  Representatives of all taxa were dried at 65°C for
24 hours and weighed for dry weight biomass.  A split  plot analysis of variance
was performed on the data to test for treatment and date-within-season effects.
Because Site II was not fumigated until 1976, we concluded it would be illogi-
cal to include "sites" and "years" in the ANOVA design.  The two sites were
not comparable in 1976 because of differences in fumigation history,  and
first-year fumigation on Site I was not comparable to  first-year fumigation
on Site II because of differences in growing seasons.   Because of high sample
variability, the ANOVA was run at the order and family level on selected
groups based on whether or not there appeared to be population changes in the
treated plots (judged on season mean density and/or biomass summaries) .
Individual analyses were performed on both density and biomass data of each
group because either or both parameters can be used to measure population
changes in a given family or order.  It should be stated at this point that
although the traditional significance level of P= 0.05 was used as a guideline
in judging population changes as significant, probability levels of 0.05 < p <
0.10 were accepted for one or more site-years for a given group if that group
showed similar trends (whether significant or not) in  other site-years.
Tukey's Q procedure was used to calculate least significant ranges which were
used to compare treatments or dates when the ANOVA results indicated  signifi-
cant population changes.  In cases where both a main effect of treatment or
date and a date-by-treatment interaction were significant,  the interaction
was given presidence over the main effect.   In most cases where this  situation
occurred, it was because the particular group was abundant only for a portion
of the season and significant treatment differences occurred at that  time.
During the remainder of the season, the group did not  occur or did so in such
low densities that treatment differences were not measurable.
                                     RESULTS

     The list of identified arthropods collected during this portion of the
study includes 15 orders and 60 families of insects,  five families of spiders
(Araneida),  five families of mites (Acarina),  and centipedes (Geophilomorpha).
A general overview of the aboveground arthropod community structure on Sites
I and II is  provided in Tables 16.1 and 16.2.   Presented are density and
biomass estimates for the major orders and families.   The major order on both
sites was Coleoptera with Hymenoptera and Homoptera following in that order
(based on biomass).   The Curculionidae (weevils) was  the major coleopteran
family, Formicidae (ants) the major hymenopteran family and the Cicadellidae
(leaf hoppers) the major homopteran family.  A complete list of all families,
genera and species is far too voluminous to include here.
                                     160

-------
TABLE 16.1.
GENERAL ABOVEGROUND ARTHROPOD  COMMUNITY  STRUCTURE OF SITE I
IN 1976*

Density (Nos • m~2)
Order
Araneida
n
Coleoptera
n
M
n
n
n
n
Collembola
n
Hemiptera
n
"
"
"
"
Homoptera
n
n
n
Hymenoptera
M
Lepidoptera
n
Orthoptera
11
Thysanoptera
n
Family

Lycosidae

Carabidae
Curculionidae
Elateridae
Staphylinidae
Tenebrionidae
Chrysomelidae

Poduridae

Cydnidae
Lygaeidae
Miridae
Nabidae
Scutelleridae

Cercopidae
Cicadellidae
Pseudococcidae

Formicidae

Noctuidae

Acrididae

Thripidae
Total Arthropods
Cont,
2.
<0.
55.
5.
10.
<0.
6.
0.
10.
173.
173.
11.
0.
8.
1.
0.
0.
50.
0.
12.
14.
22.
20.
1.
0.
0.
0.
83.
83.
420.
5
1
8
2
1
1
9
3
2
6
6
9
4
7
3
6
1
2
1
6
8
5
6
1
1
4
4
4
4
4
Low
3.3
0
44.3
4.0
10.6
0.2
4.5
0.7
7.9
6.1
6.1
14.3
0.2
10.9
1.3
0.9
0.1
21.2
0.2
14.0
4.4
27.7
25.4
0.5
0
0.4
0.3
27.8
27.8
164.1
Med.
2.9
0.2
42.3
3.5
8.2
<0.1
4.6
0.7
7.6
17.1
17.1
12.7
<0.1
9.9
1.8
0.6
<0.1
19.9
0.1
8.9
7.3
34.3
33.0
0.9
0
0.6
0.6
22.5
22.5
166.3
High
3.6
0.3
41.8
3.8
10.8
0.2
5.0
0.3
6.0
91.1
91.1
18.3
1.0
13.8
2.6
0.4
0.1
26.6
0.3
6.7
11.9
26.7
24.2
0.7
0.1
0.6
0.5
35.6
35.6
255.3
Biomass (nig
Cont.
1
0
64
7
28
<0
3
1
12
3
3
9
1
3
1
1
1
13
0
9
1
15
14
5
3
2
2
3
3
121
.6
.2
.4
.7
.5
.1
.8
.1
.0
.5
.5
.7
.6
.2
.2
.3
.2
.8
.7
.5
.3
.1
.4
.7
.4
.2
.2
.3
.3
.1
Low
1.3
0
56.8
5.5
30.0
1.5
2.3
1.7
8.8
0.1
0.1
8.8
0.8
3.2
1.3
1.9
0.7
9.9
0.8
8.1
0.4
14.0
12.9
1.3
0
3.8
1.5
1.0
1.0
98.4
. m-2;
Med.
6.3
5.0
53.6
7.5
23.9
0.1
1.7
2.3
9.6
0.3
0.3
6.5
0.1
2.8
1.5
1.3
0.3
7.7
0.5
5.7
0.7
18.3
17.4
2.0
0
8.2
7.4
0.9
0.9
105.6
)
High
5.0
3.5
62.6
7.3
29.5
2.7
2.9
1.3
11.0
1.8
1.8
12.1
3.9'
3.9
2.1
0.8
0.9
9.6
1.3
6.3
1.1
15.1
12.9
5.7
4.6
11.4
11.4
1.4
1.4
125.8
          Data are season means. The list includes groups where 1.0 mg • m~2 occurred on
          one or more treatments.
     The  three  site-year  combinations  present difficulties in analyzing and
interpreting  the  resulting  data.   As mentioned previously, first year exposure
on Sites  I and  II are  not directly comparable because they occurred in
separate  seasons  and the  only  second-year data collected were from Site I in
1976.  Because  of these problems,  potential inconsistencies between site-
years in  measured arthropod responses  to S02 fumigation could very well be
expected  and, in  fact, did  occur.   Tables 16.3 and 16.4 list those orders
and families  of arthropods  which  had trends of population density and/or
biomass changes with S0£  exposure,  based on season mean density and biomass
estimates.  Individual ANOVA's were performed for each of the groups listed.
The results will  be discussed here by  site-year.

1975 - Site I

     Total coleopteran density was reduced for part of the 1975 season
resulting in  a  significant  treatment-by-date interaction (Figure 16.1A).
This is quite probably due  to a similar  trend for the density and biomass of
                                      161

-------
TABLE  16.2.   GENERAL ABOVEGROUND ARTHROPOD COMMUNITY STRUCTURE  OF  SITE II
              IN  1976*
Density (Nos • m~2)
Order
Araneida
it
Coleoptera
11
it
ti
ti
it
"
ii
Hemiptera
11
"
Homop ter a
ii
it
Hymenoptera
it
Lepidoptera
it
Orthoptera
ii
Thysanoptera
Family

Lycosidae

Carabidae
Chrysomelidae
Curculionidae
Elateridae
Orthoperidae
Staphylinidae
Tenebrionidae

Lygaeidae
Cydnidae

Cicadellidae
Pseudococcidae

Formic idae

Noctuidae

Acrididae
Thripidae
Cont.
2
0
49
4
8
15
0
4
5
0
10
7
0
19
4
11
20
19
1
<0
0
0
31
.5
.7
.4
.3
.5
.6
.9
.6
.9
.7
.3
.7
.9
.5
.2
.9
.8
.5
.1
.1
.5
.5
.4
Low
1.
0.
53.
6.
4.
17.
1.
5.
5.
3.
14.
8.
0.
24.
4.
11.
36.
35.
1.
<0.
0.
0.
22.
4
1
6
1
6
8
8
5
0
2
0
8
2
4
2
6
6
7
5
1
7
7
2
Med.
1.7
0.1
41.3
4.2
5.3
14.8
0.5
2.9
3.0
4.0
9.7
7.8
0.1
14.9
2.3
11.0
32.8
32.4
1.2
0
0.8
0.8
23.2
High
1.9
0.2
24.4
2.4
3.2
9.8
0
2.1
3.1
1.0
9.0
5.9
<0.1
13.4
3.6
9.1
29.7
29.2
1.0
<0.1
0.9
0.8
10.3
Biomass (mg • m~2)
Cont.
3.0
1.6
80.3
7.6
14.8
47.5
2.2
1.0
3.1
2.6
10.3
2.8
3.6
5.5
3.6
1.1
9.9
9.5
2.8
1.1
1.9
1.9
1.1
Low
5.1
4.3
90.3
6.9
7.2
53.2
6.0
1.2
2.5
11.5
9.3
2.8
0.7
7.6
4.7
1.5
16.6
16.1
2.7
1.1
3.6
3.6
0.9
Med.
4.4
3.1
77 .1
7.4
7.7
42.0
1.9
0.6
1.4
14.6
6.4
2.7
0.4
5.2
3.0
1.0
14.6
14.5
1.0
0
22.3
22.3
0.9
High
6.6
5.3
40.9
2.2
4.4
28.5
0
0.5
0.9
3.2
7.2
1.7
0.1
6.1
4.4
0.8
13.2
12.8
4.0
2.3
19.8
17.4
0.4
         Total Arthropods           157.9 170.7 141.0 100.5  117.2 138.9 133.7 99.8

         "*                                                  ~
           Data are season means.  The list includes groups where 1.0 mg • m~z occurred on
           one or more treatments.
the major coleopteran family Curculionidae (Figure 16.IB).  Nine species  of
curculionid beetles were  collected on Site I in 1975 and 1976, two of which
account for over  90   percent of  the total density and biomass  for the family
Hyperodes grypidioides Dietz and E.  vittieollis (Kirby).  The E. grypidioides
was collected only in the spring and fall (probably overwintering as adults)
and E. vi-ttioollis was collected only during the mid part of the growing
season.

     Significant  treatment effects occurred for both density and biomass  for
the order Homoptera and the family Pseudococcidae.  However, the significant
reductions occurred in the Low and Medium treatments while the Control and
High plots were not significantly different from each other.  The date by
treatment interactions reveal high pseudococcid (and total Homoptera) popula-
tions on the Control  in spring and similarly high populations on the High
treatment in the  fall (data are  not presented).  Because of these erratic
trends, the population differences among the treatments are not considered
as the result of  S02  fumigation  but chance variation among the field plots.

     Although both density and biomass of the acarine family Parasitidae
were reduced in all treated plots,  none were significant because of high
sample variability.
                                      162

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TABLE 16.3.  ANOVA RESULTS FOR ARTHROPOD BIOMASS ON THREE SITE-YEARS.  NUMBERS
             ARE THE SIGNIFICANCE LEVELS FOR EACH TEST.
                                Site I - 1975   Site I - 1976   Site II - 1976
    Group                       Treat*  TxDt    Treat   TxD     Treat   TxD

Geophilomorpha                                     -     -         -    .060

Araneida       Dictinidae                                         .008  .000

Acarina (total)
    "          Tydeidae                                           .030
    "          Oribatulidae                                        -    .032
    "          Parasitidae
Collembola (total)                                 -    .007
    "          Poduridae                           -    .007
    "          Sminthuridae

Diplura

Hemiptera      Pentatomldae                       .009

Homoptera (total)                 .012   -        .003  .000
    "          Cicadellidae                       .055
               Pseudococcidae     .013  .000      .030  .001
    "          Psyllidae                           -    .000
    "          Aphididae

Thysanoptera   Thripldae                          .038  .007      .013  .071

Coleoptera (total)                 -               -    .011      .029
    "          Anthicldae
    "          Curcullonldae       -    .075
    "          Leptodiridae
    "          Staphyllnidae                                      .047

Diptera (total)                                   .089  .002
    "          Ceratopogonidae                    .007  .000
    "          Chloropidae
    "          Muscidae                           .049  .058
    11          Sphaeroceridae

Hymenoptera    Dlapriidae                                          -    .060


*  Treatment main effect.
t  Treatment by date interaction.
t  Indicates the group showed a trend of season mean population reduction with
   S02 exposure, but reductions were not significant at P < 0.10.  Blank spaces
   indicate no trends and hence not tested statistically.

                                     163

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TABLE 16.-4.  ANOVA RESULTS FOR ARTHROPOD DENSITIES ON THREE SITE-YEARS.  NUMBERS
             ARE THE SIGNIFICANCE LEVELS FOR EACH TEST.
                                Site I - 1975   Site I - 1976   Site II - 1976
    Group                       Treat*  TxDt    Treat   TxD     Treat   TxD


Geophilomorpha                                     -     ~         ~     ~

Araneida       Dictinidae                                         .008  .000

Acarina (total)                                                   .084
               Tydeidae                                           .030
               Oribatulidae                                        -    .032
    "          Parasitidae         -t

Collembola (total)                                 -    .007
    "          Poduridae                           -    .007
    "          Sminthuridae

Diplura                                                           -048

Hemiptera      Pentatomidae

Homoptera (total)                 .005  .000      .020  .000
    "          Cicadellidae
    "          Pseudococcidae     .012  .000      .032  .001
               Psyllidae                          .045  .000
    "          Aphididae

Thysanoptera   Thripidae                          .033  .004      .025  .026

Coleoptera (total)                 -    .020       -    .006      .075  .043
    "          Anthicidae
    "          Curculionidae       -    .008
    "          Leptodiridae
    "          Staphylinidae

Diptera (total)
    "          Ceratopogonidae                    .007  .000
    "          Chloropidae                         -     -
    "          Muscidae                           .048  .056
    "          Sphaeroceridae

Hymenoptera    Diapriidae                                          -    .003


*  Treatment main effect.
t  Treatment by date interaction.
t  Indicates the group showed a trend of season mean population reduction with
   S02 exposure, but reductions were not significant at P  ^  0.10.  Blank  spaces
   indicate no trends and hence not tested statistically.

                                      164

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80-|
(M

'E

L  60-

JD
   40-
co
z
UJ
Q
20-
                                   o  CONTROL

                                   x  LOW

                                   A  MEDIUM

                                   a  HIGH
                                       •-x
                                                CM
                                                 •E
                                                       lOOn
                                                    80-
                                                     E
                                                    *-  60-1
                                                    V)
                                                    o
                                                    CD
                                                       40-
                                                     20-
                                                         O-
                                                                                           1-X
                 %
 Figure 16.1.
                                           DATES  in  1975


             Time traces of  two  insect  groups on Site I in 1975.  (A) Coleoptera (Total)

             density.   (B)   Curculionidae biomass.

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1976 - Site I

     As expected, there was an increase in the number of groups showing
apparent responses to second year SC>2 fumigation on Site I.  Fifteen groups
had reductions in season mean density and/or biomass in one or more fumigated
plots  (Tables 16.3 and 16.4).  However, high sample variability again was
responsible for some of the reductions not being statistically significant,
including Geophilomorpha and two dipteran families Chloropidae and
Sphaeroceridae.  Many of the significant reductions were confused by signifi-
cant treatment-by-date interactions.  Each of these cases will be discussed
separately.

     The collembolan family Poduridae which was represented in these data by
only one species, Hyogastriwa avmata (Nicolet), had reduced densities and
biomass on all treated plots but none were significant.  However, the  treatment-
by-date interactions were significant and a plot of the biomass data
(Figure 16.2A) shows H. aimata was collected only on the first two sample
dates  at which time there were significantly smaller populations on the  ow
and Medium plots.  The High treatment was reduced but not significantly.
Certainly E. armata is not the only collembolan occurring on the field
plots, but it is the major species occurring on the soil surface in late
winter and early spring.  It often is found in large numbers on or near
water  puddles.

     One hemipteran family,  Pentatomidae,  represented largely by Neoti-glossa
sulc'Lfvons Stal. late in the growing season,  had significantly reduced
season mean biomass on the Medium and High treatment plots (Figure 16.3A).
The order Homoptera had significant treatment effects for both density and
biomass, however, in both cases there also were significant interactions.  A
plot of the density data (Figure 16.2B),  which is similar to that for biomass,
shows  a significant late season increase in the populations on the Control
plot while similar increases did not occur in any treated plot.  The families
Cicadellidae and Pseudococcidae made up a majority of the Homoptera.  The
cicadellids had significantly reduced biomass on the Medium and High treatments
(Figure 16.3B).  Numerous genera and species of cicadellids were collected
thoughout the season with various seasonal abundance patterns.  The population
reductions appeared not to be the result of one major species being affected
but a general reduction of most of the dominant species.  Only one species
of pseudococcid was collected (Distiohli-ooaous sp.)  and it occurred throughout
the season.  It had significantly reduced densities and biomass on the low
and Medium plots on the first sample date as determined from the interaction.
Trends were quite erratic and possibly not a reflection of S02 fumigation.
The family Psyllidae had reduced biomass and densities on all treated plots
late in the season, but the only significant treatment differences occurred
on the fifth sample date (Figure 16.2C).   No representatives of the only
genus  collected, Craspedolepta, were collected in any treated plot after the
third  sampling.

     Both density and biomass of Thripidae (Thysanoptera)  were reduced late
in the season.  Significant treatment differences occurred only on the fifth
date (Figure 16.2D), where all treatments were significantly lower than the
Control , however a trend of reduced populations in all treatments occurred
across the last four sample dates.  At least eight species of thrips, all of

                                     166

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      2.5-1
                                         160-1
                             DATES
                                        1976
Figure 16.2.
Time traces of five  insect  groups on Site I in 1976.  (A)
Poduridae (Collembola),   (B)   Homoptera (Total),  (C)
Psyllidae (Homoptera),   (D)   Thripidae (Thysanoptera),  (E)
Diptera (Total)-
                                     167

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                                   Jl
0.15-



c
0.10-
0.05-
tNI M n o.oo-




CID CONTROL
ESLOW
IZ3 MEDIUM
C3HIGH
d


                                     TREATMENTS
Figure 16.3.
Season mean biomass of four insect groups on the four treat-
ment plots of Site I in 1976.  (A)  Pentatomidae (Hemiptera),
(B)  Cicadellidae (Homoptera),  (C)  Ceratopogonidae (Diptera),
and  (D)  Muscldae (Diptera).
 the family Thripidae, were collected, only two of which were identified  to
 genus - Chirothrips sp. and FTarikl'in'iella sp.  Neither of these  two  species
 were of major importance among those collected.  Four other species  comprised
 the majority of  the thrip biomass and they were generally most abundant  in
 the last half of the season.

     Significant treatment-by-date interactions for total Coleoptera density
 and biomass resulted when the Control differed from the Medium treatment on
 the third date and the Eigh treatment on the fifth date (data not  presented).
 No other significant treatment differences occurred which suggests the
 differences were chance happenings.

     The significant treatment-by-date interaction for total dipteran biomass
 resulted when the High treatment was significantly lower than the  Control on
 the first sample date and all treated plots were lower than the  Control  on
 the fourth date  (Figure  16.2E).  As with the total Coleoptera, there are no
 consistent trends across all dates, so it becomes questionable if  the two
 significant points represent treatment differences.  Both dipteran families
 with significant population reductions, Muscidae and Ceratopogonidae, were
 collected in the larval stages from the soil surface litter.  Fannla sp.
 (Muscidae) was collected on only two sample dates (17 May and 12 July) and
 the ceratopogonid (species unidentified) were collected from all treatments
 on 22 March 1976 but only from the Control plot on 17 May and was  not collected
                                       168

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from any of the plots during the remainder of the season  (Figures 16.3C and
 16.3D).  The significant interactions were the result of the temporary
occurrence on the plots and not from erratic seasonal trends.

1976 - Site II

     First year fumigation on Site II resulted in more groups showing popu-
lation changes than occurred during the first year on Site I.  However,
again because of high sample variability some of the changes were not signi-
ficant including Sminthuridae (Collembola), Homoptera (total), and Leptodiridae
(Coleoptera).  Each of these groups showed trends of density and/or biomass
reductions in the treated plots, based on season means.

     A plot of the treatment-by-date interaction for centipedes (Geophilo-
morpha) shows erratic collections in the first half of the season with no
collections thereafter (Figure 16.4A).  The most consistent characteristic
is that no representatives were taken in the High treatment plot and very
few in the  edium treatment.  However, considering the reductions as being
the result of S02 fumigation is tenuous.  One family of spiders (Dictynidae),
represented by Di,ctyna oonsutta Gertch and Ivie and D, terrestr-i-is Emerton
had significantly reduced density and biomass in the Medium and High treat-
ment plots on- the third sample date and in all treated plots on the fifth
sample date (Figure 16.4B).  Total acarine density was reduced on all treated
plots although the significance level was only P = 0.084  (Figure 16.5A).  The
density and biomass of the acarine family Tydeidae was significantly reduced
on all treated plots (Figure 16.5B).  A plot of the date by treatment inter-
action for Oribatulidae biomass shows a significant reduction on the fifth
sampling when populations were at their highest (Figure 16.4C)„  The density
of Diplura was reduced on all treated plots, however, the reduced biomass
was not significant (Figure 16.5C).

     Both density and biomass of Thripidae (Thysanoptera) were significantly
reduced on the High treatment plot (Figure 16.5D) although the significant
interaction shows the reduction occurred late in the growing season much the
same as on Site I.  Total beetle (Coleoptera)  biomass was significantly
reduced on the High treatment plot (Figure 16.5E) while a significant inter-
action occurred for density.  A plot of the interaction (Figure 16.4D)  shows
the High treatment to be consistently lower than the Control, Low, and
Medium plots, but that significant differences occurred on the third, fifth,
and sixth dates.  Only one coleopteran family, Staphylinidae, had a signifi-
cant biomass reduction, where both the Medium and High treatments were
reduced from the Control (Figure 16.5F).  Three species made up the majority
of the Staphylinidae - Philonthus sp., Aleochara sp., and Taohyporus sp.
The Philonthus was collected throughout the season while the Aleookara sp.
and Tachyporus were collected almost exclusively in the first three samplings.
At least six other species were collected but only rarely.  The reduction in
Staphylinidae was due to reductions in all three of the principal species.
One other coleopteran family, Curculionidae, showed substantially reduced
biomass on the High treatment, but the data were untested.

     One parasitic hymenopteran family, Diapriidae, showed significant
interactions for both density and biomass, particularly density (Figure 16 .4E).

                                     169

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0.8-1
                    o CONTROL
                    X LOW
                    A MEDIUM
                    D HIGH
                             0.8
     \   '\\\\**<
                                >
>
0.4-,
                      DATES in 1976
Figure 16.4.
     Time traces of five  arthropod groups on four treatment plots
     of Site II in 1976.  (A)  Geophilomorpha,   (B)  Dictynidae
     (Araneida),  (C)   Oribatulidae (Acarina),   (D)  Coleoptera
     (Total),  (E)  Diapriidae (Hymenoptera).
                          170

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Figure 16.5.
                    TREATMENTS

Season mean density or biomass of six arthropod groups on four
treatment plots of Site II in 1976.  (A)   Acarina,   (B)
Tydeidae (Acarina),  (C)  Diplura,  (D)   Thripidae  (Thysanoptera),
(E)  Coleoptera (Total),  (F)  Staphylinidae (Coleoptera).
The reduction occurred early in the season when they were most abundant.  No
species identifications were made.

                                  DISCUSSION

     All arthropod population changes noted here as associated with S02
fumigation have been reductions in density and/or biomass.  No significant

                                      171

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population increases were observed for any group in any season although
increases certainly could have been expected as a result of upsetting predator-
prey balances or changes in plant host susceptability.  Both concepts have
been argued as causes of increased insect damage to plants in areas of high
air pollutant exposure (Hillman and Benton, 1972; Heagle, 1973) .

     Although numerous groups showed significant population reductions
associated with the S02 fumigation in the three site-years, we are concerned
over the lack of consistency between sites and years.   Only three groups had
significant population reductions in more than one site year.  Total homopteran
density and biomass were significantly affected in 1975 and 1976  on Site I;
the family Thripidae was significantly affected on both sites in  1976; and
total coleopteran density and biomass were variously reduced in all three
site-years.  All other groups that showed population changes did  so in only
one site-year.  As stated previously, these inconsistencies were  not completely
unexpected because of the way the field study was designed and implemented,
*i.e. , first year fumigation on the two sites being in different seasons and
only one set of second season data.  Despite these inconsistencies, there
are enough significant population reductions and trends of such to lead to
the conclusion that S02 fumigation did have detrimental effects on many
aboveground arthropod groups and that the reductions were not chance occur-
rences among a large number of groups.

     The treatment responses of arthropods to long-term low-level S02
exposure observed here fall into two general categories - 1) those arthropods
(or stages) which are associated with the soil surface litter and relatively
non-mobile, and 2) those arthropods associated with aerial vegetation and
generally quite mobile.  The former group includes the Geophilomorpha,
Araneida, Diplura, Acarina, Poduridae, Pseudococcidae, Muscidae (larvae) and
Ceratopogonidae (larvae).  The latter group includes the Cicadellidae,
Thripidae, Staphylinidae, and Curculionidae.  Direct toxicity or  toxicity to
food resources would conveniently explain the population reductions in the
first group simply because those organisms cannot leave the plots for mere
avoidance of the S02.  A possible exception here would be the two dipteran
families where the population reductions could be the result of avoidance of
the treated plots by the adults during oviposition.  Since all of the members
of the first group were found to occur in the soil surface litter it is
quite possible to link their population reductions to other determined
effects of S02 on the litter, i,e., reduction of decomposition rates of
plant litter as a consequence of reduced microbial activity (Leetham et al.,
submitted a; Dodd and Lauenroth, 1980).  Decreased microbial activity may re-
flect decreased available microbial food reserves for arthropod groups listed,
most of which are considered to be utilizing these resources wholly or
partially.  Certainly direct toxicity is a real possibility for explaining
population decreases in all the arthropods since other studies have shown
S02 can be toxic in relatively small concentrations (Lebrun et at., 1977;
Ginevan and Lane, 1978).

     The fact that many of the population reductions in litter inhabiting
groups occurred in the early part of the growing season was not unexpected
since it is well known that S02 is highly attracted to moist surfaces (Saunders,
1966; Hocking and Hocking, 1977) and S02 toxicity to arthropods can be

                                      172

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increased with relative humidity  (Lebrun et al., 1978).  The soil moisture
conditions are wettest in the spring and early  summer  (Dodd et al., 1978).

     Another important possible explanation for the reduction in populations
of the more mobile arthropod groups (listed in  group two previously) on the
fumigated plots may involve behavioral avoidance.  Since ea-.h treated plot
was only 0.52 ha in size, groups  such as Staphylinidae, Curculionidae,  and
Thripidae, which are active fliers, could easily move out of the plots or at
least not move into them in their various random movements.  Under control
conditions, the population of a given species of active arthropod in a given
small plot of ground may be maintained by a rough balance of emigration and
immigration.  This balance could be upset if individuals are repulsed by the
presence of S02 and hence avoid the plots in their random flight movements.
Bromenshenk and Gordon (1978) using the same field sites as this study have
shown that the dung beetle Canthon sp. (Scarabaeidae) could not be attracted
to carrion baits in the S02 treated plots in the densities attracted to
similar baits on the Control plots (both sites).  The differences were
significant and suggest that the beetles' behavior was influenced by the
S02.  The critical factor in this explanation is the size of the field
plots.  The effect of S02 on the active arthropod groups may be quite differ-
ent if a large enough region were exposed so as to rule out behavioral
avoidance of the polluted atmosphere.  Normal behavioral patterns may or may
not be affected to the extent of significantly changing the population size
and/or dynamics of a given arthropod species.  Hillman and Benton (1972)
found reduced foraging activities of honey bees when exposed to S02 in low
concentrations of 100 to 600 pphm.  The resolution of this question remains
to be made.

                                 CONCLUSIONS

     Significant population reductions in density and/or biomass were observed
on S02 treated plots during the two-season study although the reductions
were not large enough or involve enough of the dominant groups to cause a
significant change in tha overall total aboveground arthropod population
estimated of either site.  The arthropod groups which showed significant
density and/or biomass changes are listed in Tables 16.3 and 16.4.   Inconsis-
tencies between site-years are cause for concern about the extent of the
effects of S02 fumigation.  However, the numerous significant population
reductions are accepted as evidence that S02 did have a deleterious effect
on the above ground arthropod community.

     The arthropods listed in Tables 16.3 and 16.4 can be generally categorized
into two groups.  One group would include the relatively immobile types that
are strongly associated with the soil surface litter (Acarina, Diplura,
Collembola, and Diptera larvae).  The other group would include the relatively
mobile, flying insects which may only partially be associated with the
surface litter or not at all.  The former group members possibly are reduced
by direct toxicity of S02 or toxic effects on food resources or a change in
soil acidity.  The second group, in addition to being affected by toxicity
(direct or indirect), may also be reduced by behavioral changes due to S02
which may result in a change in emigration/immigration ratios, i.e,, avoidance
of the relatively small field plots.  There is published evidence to support

                                      173

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both concepts,  but our data are not definitive enough to  conclude if  either
or both mechanisms were involved.

                                   REFERENCES

Bromenshenk, J. J. and C.  C. Gordon.  1978.   Terrestrial  Insects Sense Air
     Pollutants.  In:   Conference Proceeding, Forest Joint Conference on the
     Sensing of Environmental Pollutants,  1977.   Am. Chem. Soc., Wash., D.C.
     pp. 66-70.

Dodd, J. L., J. W. Leetham,  T. J.  McNary,  W.  K.  Lauenroth, and  G. L.  Thor.
     1979.  Baseline Characteristics of Producer and Invertebrate Populations
     and Certain Abiotic Parameters in the Colstrip Vicinity.   In: E. M.
     Preston and T. L. Gullett (eds.) The  Bioenvironmental Impact of  a Coal-
     Fired Power Plant, Fourth Interim Report.  EPA-600/3-80-044.  U. S.
     Environmental Protection Agency, Corvallis, Oregon,  pp.  53-106.

Dodd, J. L., and W. K. Lauenroth.   1980.  Effects of Low Level  S02 Fumigation
     on Decomposition of Western Wheatgrass Litter in a Mixed-grass Prairie.
     In:  E. M. Preston and D. W.  O'Guinn  (eds.)  The Bioenvironmental Impact
     of a Coal-Fired Power Plant,  Fifth Interim Report.   EPA 600/3-80-052.
     U.S. Environmental Protection Agency, Corvallis, Oregon, pp. 212-215.

Freitag, R., L. Hastings,  W. R. Mercer,  and A. Smith.  1973.  Ground  Beetle
     Populations Near a Kraft Mill.  Can.  Entomol.,  105:299-310.

Ginevan, M.  E.  and D.  D. Lane.  1978.  Effects of Sulfur  Dioxide in Air on
     the Fruit Fly, Drosophila melanogaster.   Environ.  Sci.  Technol., 12:821-
     831.

Heagle, A. S.  1973.  Interactions Between Air Pollutants and Plant Parasites.
     Ann. Rev.  Phytopathol., 11:365-388.

Hillman, R.  C.  and A.  W. Benton.  1972.  Biological Effects  of  Air Pollution
     on Insects, Emphasizing the Reactions of the Honey Bee  (Apis metl-ifeva
     L.) to Sulfur Dioxide.   J. Elisa Mitchell Sci.  Soc., 88:195.

Hocking, D.  and M. B.  Hocking.  1977.  Equilibrium Solubility of Trace
     Atmospheric Sulfur Dioxide in Water and  its Bearing  on  Air Pollution
     Injury to Plants. Environ. Pollut., 13:57-64.

Lebrun, P ., G. Wauthy, C .  Leblanc, and M. Goossens.  1977.  Ecologic Test
     of the Tolerance to S02 Toxicity in the  Oribatid Mite EwneTobates
     rostrolamellatus (Grandjean,  1936)  (Acari:0ribatei)  Annales Soc. r.,
     Zool.,  Belg., 106:193.

Lebrun, p ., J. M. Jacques,  M. Goossens, and  G.  Wauthy.   1978.   The Effect
     of Interaction Between the Concentration of S02 and  the Relative Humidity
     of Air on the Survival of the Bark-living Bioindicator  Mite Himevobates
     rostrolamellatus.  Water, Air, and Soil  Pollu., 10:269-275.
                                     174

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Leetham, J. W.  1975.  A Summary of Field Collecting and Laboratory Processing
     Equipment and Procedures for Sampling Arthropods at Pawnee Site.  U.S./
     IBP Grassland Biome Tech. Rep. 284.  Colorado State Univ., Ft. Collins.
     49 pp.

Leetham, J. W., J. L. Dodd, and W. K. Lauenroth.  Effects of Low-Level Sulfur
     Dioxide Exposure on Decomposition of Western Wheatgrass (Agropyron
     smith-ii.) Litter Under Laboratory Conditions. (Submitted a).

Leetham, J. W., J. L. Dodd, R. D. Deblinger, and W. K. Lauenroth.  Arthropod
     Population Responses in Three Levels of Chronic Sulfur Dioxide Exposure
     in a Northern Mixed-grass Ecosystem.  I.  Microarthropods. (Submitted b).

Saunders, P. J. W.  1966.  The Toxicity of Sulfur Dioxide to Diploaarpon
     rosae Wolf Causing Blackspot of Roses.  Ann. Appl. Biol., 58:103<-114.
                                     175

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                                  SECTION 17

        RESPONSE OF MELANOPLUS SANGUINIPES  TO  LOW-LEVEL  SULFUR DIOXIDE
            EXPOSURE  FROM EGG HATCH TO  ADULT  (ORTHOPTERA:ACRIDIDAE)

          J. W.  Leetham,  J.  L. Dodd,  J.  A.  Logan,  and  W. K.  Lauenroth
                                   ABSTRACT

               The effects of  low-level  S02 exposure  on the
          migratory grasshopper Melanoplus  sanguini-pes  (Fab.)
          from egg hatch to egg-laying adult were  investigated
          by rearing the grasshoppers  in controlled laboratory
          environments.   A nondiapausing strain of M. sangu-inipes
          was reared from eggs in control and S02  environments,
          the S02 concentration being  17 pphm (468 yg • m~3).
          No significant difference in egg-hatching success,
          mean developmental time for  each  nymphal instar,  adult
          dry weight biomass,  and egg  production per  female per
          day were found between  control and S02-exposed indivi-
          duals.   There  was, however,  a  significant reduction  in
          the variability around  the mean developmental time for
          instars three,  four,  and  five  in  the  S02~exposed  nymphs.
          At the  same time,  there was  evidence  of  increased
          mortality of S02~exposed  nymphs.   It  is  postulated that
          the physiologically  marginal individuals of a given
          instar  are more vulnerable to  the S02  stress  and  hence
          are eliminated  rather than continue to develop  slower
          than the remaining members of  the same instar.  There
          were more slower-developing  third,  fourth,  and  fifth
          instar  nymphs  in the control group.
                                 INTRODUCTION

     Studies of the direct toxicity of S02 on arthropods are few and
generally do not address the question of the effects of realistic
atmospheric S02 concentrations on arthropod survival.  For example, Weedon
et al,  (1939) studied the deleterious effects of very high S02 concentra-
tions on various vertebrate and invertebrate animals.  They calculated an
LD50 for the grasshopper Melanoplus differentialis (Thomas) at 10700 pphm
for 5 days.  Sulfur dioxide has been shown to be effective in high concen-
trations as an insecticide for stored-grain insect pests (Kanaga, 1956).
                                     176

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     Only a few studies have been concerned with low-level S(>2 exposure on
arthropods.  Hillman and Benton (1972) found reduced brood rearing and
pollen collection in honey bee (Apis mellifera L.) colonies fumigated with
SC>2 concentrations of 0 to 500 pphm over 9- and 14-week periods.  Ginevan
and Lane (1978) found increased developmental times and decreased survivability
of fruit flies (DTOsophila metanogastev Meigen) exposed to 40 and 70 pphm
S02 during the larval stage.  Lebrun et at. (1977) found Ewnerobates
rostrolamellatus (Grandjean), a bark-living oribatid mite, very sensitive to
S02.   Exposure to 45 pphm for 2 days resulted in 50 percent mortality in experi-
mental populations.  All of these aforementioned three studies used S02
concentrations much higher than generally encountered even in highly polluted
areas which makes the results questionably applicable to real life situations.

     This study was undertaken in hopes of clarifying the results of a field
study of the effects of low-level, long-term S02 exposure on rangeland
grasshoppers in southeastern Montana (McNary et at., submitted).  In that study
season-long exposure of field plots of native northern mixed-grass prairie
were exposed to controlled levels of SC>2 of less than 10 pphm (260 yg • m~3)
throughout the growing season (April-October).  Significantly reduced
grasshopper populations were found, especially for the species M, sangui-n-
ipes  (Fab.)-  The mechanism by which the populations were reduced was
not resolved between direct toxicity and behavioral changes.  The field
plots were relatively small (0.52 ha), which would have allowed the grass-
hoppers to leave the area, or at least not enter the area, because of
repulsion by the S02.  This study was performed to test for direct toxicity
of S02 to a laboratory strain of M. sanguinipes reared under continuous S02
exposure from egg hatch to egg-laying adult.

     The dynamics of nymphal development and nymphal mortality were of prime
interest in this study.  Low-level, chronic toxicant exposure may affect
developmental rates in two ways.  Median time to complete an instar may be
altered and/or the variation in developmental rates may be affected.  Modifi-
cation of either the time required to complete a stadium or the variation in
developmental rates may have profound ramifications upon an organism's total
life system.  Taylor (1980) discussed in detail the importance of timing
critical life history events in insect population dynamics.  Stinner et at.
(1977) discussed the importance of accurately representing variation in life
history events.  They further presented an example of variation in develop-
mental rates dramatically affecting individual fitness in a Hetiothi-s zea
(Boddie) population.

     Also of interest in this study were adult dry weight biomass (newly
emerged) and egg laying success, since both parameters are indicators of the
fitness of the individuals within a population.  We hypothesized that S02
effects on such parameters as food intake rate, digestion rate, and as-
similation efficiency would be reflected in the ultimate size and/or egg
production of adults.  If either, or both, parameters are measurably affected
by S02 exposure, major population level change would be expected.
                                      177

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                             MATERIALS AND METHODS

     This study was conducted at the headquarters buildings of the field
research site of the Natural Resource Ecology Laboratory.  Since the site is
approximately 35 miles northeast of Fort Collins, Colorado, in the Pawnee
National Grasslands, it afforded relatively clean ambient air that could be
used without scrubbing.  Also, the ambient relative humidity is very low,
eliminating the need to artificially lower the humidity before circulation
through the exposure chambers.  Low humidity is considered critical for
successful laboratory rearing of the grasshoppers used in this study.

     The exposure chambers used were simple continuous-flow, single-pass
cabinets measuring 2 ft by 2 ft by 6 ft (61 cm x 61 cm x 183 cm).  They were
constructed completely of V (0.64 cm) clear plexiglass with large side-
opening doors for easy access.  Air movement through the chamber was at an
approximately linear velocity of 0.46 to 0.91 m • min  , resulting in a com-
plete air turnover once every 1 to 2 minutes.  The chamber inlet and exhaust
fans were set up to create a slight negative internal pressure to prevent
pollutant leakage.  Source SC>2 was fed directly into the inlet air stream.
Details of the chamber construction and operation are given by Leetham et-
a.1.  (submitted).  Sulfur dioxide concentration was maintained at 17 pphm through-
out the study.  Measurement of the SC>2 was by two methods.  A flame photometric
sulfur gas analyzer (Meloy Laboratories, Inc., Model SA-160) was used to get
accurate point measurements at the outset and conclusion of the study and
occasionally during the interim.  For continuous monitoring, a technique of
chemical absorption (Pararosaniline method) was used to give average concen-
trations over time (CFR, 1975).

     Rearing and adult maintenance was in clear acetate tubes of two sizes,
capped with aluminum screen-covered lids.  Large tubes (9 cm diameter x 51 cm
long) were used for egg hatching and nymphal development, while smaller
tubes (5 cm dia. x 20 cm long) were used to pair adults for egg production.
The large tubes were held horizontally on an aluminum rack, while the small
tubes were held vertically in moist sand within a styrofoam cup.

     Two exposure chambers, control and S02, were housed in a temperature-
controlled room maintained at 35°C.  Relative humidity was uncontrolled but
averaged 5-15 percent throughout the study except when passing storm fronts
temporarily elevated the humidity.

     A nondiapausing strain of M. sanguln-ipes was used for this study.  Eggs
were obtained from the Range Insect Laboratory, Montana State University,
Bozeman, where a disease-free culture is maintained.  The strain was originally
developed at the Saskatoon Research Station of the Canada Department of
Agriculture (Pickford and Randall, 1969).  Eggs were maintained in moist
vermiculite until hatch.  All life stages were fed a diet of head lettuce
and a dry-mix medium composed of 50 g alfalfa meal, 50 g wheat midlings, 25
g soybean meal, 5 g brewer's yeast, and 11.5 ml corn oil.

     The study was initiated by placing eight groups of eggs numbering 100
to 200 eggs per group in each chamber 7 days prior to hatching to test
hatching success and to ensure that the nymphs received the desired exposure

                                     178

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from the moment of hatching.  All newly hatched nymphs were counted at 24-hr
intervals, at which time groups of 20 were placed in the larger acetate
tubes for rearing to the adult stage.  This ensured that the nymphs were all
nearly the same age in any given group of 20, making determination of develop-
ment stage easier.  A total of 16 groups of 20 nymphs were placed in each
chamber.  At 48-hr intervals, each group of 20 nymphs was evaluated for
instar structure and mortality until all survivors reached adulthood.  From
the surviving adults, male-female pairs were set up in the small acetate
tubes for egg production.  A reserve of males was maintained to replace
those that died before the female died.  A total of 48 excess male and 48
excess female adults from each chamber were killed by freezing, dried at
65°C for 24 hr and weighed.  Egg pods were retrieved and counted at 48-hr
intervals.  Moist sand from an ephemeral stream bed was used for the oviposi-
tion medium.  All eggs laid were counted but not maintained for second-
generation studies.  Egg-laying was continued for 41 days, with 32 pairs in
each chamber at the outset.

     A preliminary trial study was performed with just eight groups of 20 nymphs
in each chamber.  Only nymphal mortality and adult egg-laying success data
are included here.

     Simple t-tests were used to compare the precent egg hatch in each
chamber and, at the end of the study, to compare the mean number of eggs per
female per day in each chamber.  A paired t-test was used to compare mortality
rates while a two-way factorial ANOVA (treatment, sex) was used to compare
dry weight biomass data.  For the developmental data a probit analysis
(Finney, 1971) provided a means for testing the effect of the low-level S02
atmosphere on both median and variance in developmental rate (rate of
development = I/time to complete a life stage).  A probit transformation was
made for the cumulative percent of individuals completing each instar.
Because experimental replicate (tubes) were treated identically within
treatment and replication was entirely a function of experimental convenience
(.i.e. > the grasshoppers were confined in plastic tubes to facilitate counting),
the replicates were pooled and probits were computed for the total treatment
population.  Sample size varied from 250 to 320-  The transformed data were
then regressed on the elapsed time (from eclosion) to completion of an
instar.  Median (M) time to completion of an instar was then computed as

                              m = £ (5 - I)                           (1)

where b is the slope from the regression line and I is the y-intercept.  The
standard deviation in time to completion of an instar was estimated from
                                                                      (2)
                                       p
                            RESULTS AND DISCUSSION

      The percent hatch was  similar for the  Control and  S02—71.8 percent  (S.D.  =
 18.0  percent) and  67.4 percent  (S.D. = 12.6 percent), respectively.  The  slight-
 ly  reduced rate in the S02  chamber was not  significant  (P = 0.05).   These per-
 centages compare favorably  with those  (55-80 percent) of Pfadt et al.  (1979),
 who used the same  strain.   They also compare favorably  with the 53-77 percent

                                       179

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found by Pickford (1960),  who used a wild strain of the same species.   The fact
that the eggs were not maintained under treatment conditions throughout their
embryological development  confounds the apparent lack of SC^ effect.

      From the probit  analysis  confidence intervals  about median  development
 times indicated  no statistically significant  difference between  control and
 S02 nymphs,  and  no observable  trends  existed  in median developmental  times.
 An analysis  of covariance for  homogeneity of  regression coefficients,
 however,  indicated that the  difference between  control and  treatment  variance
 in developmental rates was highly significant (P <  0.05) for  the third,
 fourth,  and  fifth instars.   Data are  summarized in  Table 17.1.

      The variation in developmental rates is  significantly  and consistently
 reduced in the S02-treatment group  (Table 17.1).  A possible  biological
 interpretation of the reduction  in  variation  of developmental rates is that
 physiologically  marginal  individuals  are adversely  affected by the S02
 atmosphere.   This interpretation may  be logical if  the assumption that
 physiologically  less-fit  individuals  exhibit  a  retarded developmental rate
 under normal  circumstances is  valid.   If so,  it follows that  these physio-
 logically less-fit individuals would  be less  likely to withstand the  addi-
 tional stress of S02  intoxication.  This interpretation is  consistent with
 the observed trend of reduced  survival in the S02-treatment group (Figure
  17.1).   Further circumstantial  evidence to support the conjecture that
 reduced variation is  the  result  of  increased  mortality of slow-developing
 individuals  was  gained by performing  an analysis for the fifth instar,
 ignoring  the  end  point (100 percent-completed life  stage)  for the Control group.
 When  the  end  point  (i.e.,  those  individuals with  the most retarded developmental
 rates) was ignored, no significant difference was found between  the Control and
 treatment groups.

      The trend of increased  mortality in the  S02 nymphs appears  to support
 the significant  reduction in the variation around the mean  developmental
 time for the latter instars.   Mortality data  for both trials  were tested
 with a paired t-test.  In both trials mortality rates were  significantly
 greater in the S02-exposed grasshoppers (P =  0.001  in both  trials).   Total
 mortality was a  bit greater  in the  first trial  (36.9  and 41.2 percent  for
 Control  and  S02,  respectively) than in the second (30 percent in both Control
 and S02,  respectivlly) than  in the  second (30 percent in both control  and S02).
 These figures compare  favorably  with  the 35-39  percent mortality found by Pfadt
 et al.  (1979)  using the same strain of grasshopper  and nearly the same rearing
 conditions.   The rearing  conditions other than  S02  appear not to have  been
 stressful on  the nymphal  instars  such that greater  than normal mortality oc-
 curred.
      Pfadt et al. (1979)  concluded  that rearing temperature had  a substantial
 effect on the number  of nymphal  instars that  M.  sanguinipes may  have.   Six
 instars usually  result when  rearing temperatures are below  30°C, and  five is
 common when  the  temperatures are over 30°C.   In their study,  97% of the
 females and  51%  of the males had six  instars  when reared at 30°C.  In this
 study we found that all grasshoppers  had five instars.  Our rearing tempera-
 ture was 35°C.
                                      180

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       TABLE  17.1.  PROBIT ANALYSIS OF DEVELOPMENTAL DATA
00

Ins tar
3
4
5
5
Treatment
Control
S02
Control
S02
Control
S02
Control**
S02
n
6
6
8
10
6
8
5
8
I
-0.760
-6.279
-1.746
-6.144
-5.557
-10.816
-8.388
-10.816
b*
0.4441
0.8811
0.4092
0.6094
0.4111
0.5924
0.5160
0.5924
r2
0.90
0.99
0.95
0.98
0.95
0.96
0.99
0.96
m
12.97
12.80
16.49
16.84
25.67
26.70
25.95
26.70
s
2.25
1.13
2.44
1.64
2.43
1.69
1.94
1.69
P
0.0066
0.0013
0.0270
0.2642

n = number
P = probab:
of days.
Llity of obtaii

ling

the observed

difference

in standard

deviations

by pur

e
            chance  (0.05 =  5% rejection).

       *    Note  that m is  computed from the probit relationship given in equation (1).  The
            apparent inconsistency of  increasing the median number of days to completion of the
            fifth instar control by ignoring the end point is due to an artifact in estimation
            from  the probit equation.

       **   End point of retarded individuals ignored.

-------
           m
           D
           o
           cr
           LJ
           CD
           |X
               20
               18
           CO
           IE
           LJ
           0-
           CL.
           O
           I
           CO   |C
           CO   l6
           IE
           IT
           LJ

           H
               14
               12
                        Control
                 \\	18 pphm S02
                  4  8  12  16  20  24  28   48   12  16  20  24  28  I   5
                         FEBRUARY                    MARCH         APRIL

Figure  17.1.   Grasshopper survival  through  five nymphal instars to  adult
               under  control and  S02  exposure.   A = preliminary trial,
               B = second trial.
     For adult dry weight no  significant  treatment  effect was found (P =
0.05); however, as expected,  there was  a  highly  significant (P = 0.001)
difference between sexes.  No  significant interaction occurred.  Apparently
none of the parameters of food intake rate, digestion,  and assimilation
efficiency were substantially  affected.

     Egg-laying success for adult females was  poor  compared with data from
Pfadt et al.  (1979).  They found that for adult  females held at 30°C and fed
a diet similar to that used in this study, an  average of 6.7 eggs were
produced per  female per day.   Smith (1966) found an even higher average
(9.4) for a wild strain of M.  sangu-inipes.  In this study,  eggs laid per
female per day in the preliminary trial was 0.90 for both control and S02-
exposed females.  In the second trial,  there was an increase to 2.3 and 2.0
for the control and S02-treated females,  respectively.   The low egg production
resulted from fewer eggs per pod rather than a reduction in the number of
pods per female.  The fact that egg-laying in  both  trials was not carried
out to completion for all females may have influenced the above calculations.
No significant (P = 0.05) reduction in  egg production was found in either
trial.  The S02 exposure apparently did not confound or add to other,  undeter-
mined causes  for the overall reduced egg  production.

     The results of this study help in part to resolve  the  reason for  reduced
populations of M.  sanguinipes  in the field study by McNary  et al.  (submitted).
However, the  implications are  such that,  unless  S02  has greater effects on
                                     182

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subsequent generations, the increased mortality found here would eliminate
only the marginally fit individuals from a population, leaving the healthy
individuals to produce an egg supply not substantially different from an
unexposed population.  In addition, the reduction of some individuals could
decrease the intraspecific competition for the remaining individuals.  The
net result is the maintenance of a field population under regional air
pollutant impact much the same as in a similar, unpolluted area.  The critical
question left unanswered by this study is whether S02 can have cumulative
effects over numerous successive generations of M.  sangui-nipes or any other
insect species.

                               CONCLUSIONS

     Low-level S02 exposure of the migratory grasshopper M.  sanguinipes
from egg hatch through egg-laying adult did not cause large effects on most
of the parameters of the life cycle measured, including egg-hatch success,
rate of nymphal development, adult weight, and adult egg production.   Sulfur
dioxide did cause a reduction in the variability around the mean developmental
time for instars three, four, and five, possibly by increasing mortality in
physiologically marginal nymphs.  An apparent increase in mortality rate was
observed in both trials.  Except for egg-laying success, the general rates  of
the parameters measured in this study agree with those of other life history
studies of the same species.

                               REFERENCES

Code of Federal Regulations, Title 40, Protection of Environment.  Part
     50.11, July 1, 1975.  Office of the Federal Register, General Services
     Administration, Washington, DC.

Finney, D. J.  1971.  Probit Analysis.  Cambridge University Press, Cambridge.
     333 pp.

Ginevan, M. E., and D. D. Lane.  1978.  Effects of Sulfur Dioxide in Air on
     the Fruit Fly Drosophila melanogaste?.  Environ. Sci. Technol.,  12:828-
     831.

Hillman, R. C., and A. W. Benton.  1972.  Biological Effects of Air Pollution
     on Insects, Emphasizing the Reactions of the Honey Bee (Apis mellifera
     L.) to Sulfur Dioxide.  J. Elisha Mitchell Sci. Soc., 88:195.

Kanaga, E. E.  1956.  An Evaluation of the Use of Sulfur Dioxide in Fumigant
     Mixtures for Grain Treatment.  J. Econ. Entomol., 49:723-729.

Lebrun, P., T. Wauthy, C. LeBlanc, and M. Goossens.  1977.  Ecologic Test
     of the Tolerance to S02 Toxicity in the Oribatid Mite EimeTobates
     Tostrolamellatus (Grandjean, 1936)  (Acari:0ribatei).  Annales Soc. R.,
     Zool., Belg., 106:193.

Leetham, J. W., W. Ferguson, J. L. Dodd, W. K. Lauenroth.  Design and
     Construction of a Simple, Continuous-flow Sulfur Dioxide Exposure
     Chamber.  (Submitted.)

                                     183

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McNary, T. J., D. G. Milchunas,  J.  W.  Leetham, W. K. Lauenroth,  and J. L.
     Dodd.  The Effect of Controlled Low Levels of SC>2 on Grasshopper
     Densities on a Northern Mixed-grass Prairie.  (Submitted.)

Pfadt, R. E.,  Y. Afzali,  and J.  S.  Cheng.  1979.   Life History and Ecology
     of the Nondiapause Strain of the Migratory Grasshopper in the Laboratory.
     Univ. Wyo. Agric. Exp.  Sta. Sci.  Monogr.  39, Univ. Wyoming, Laramie.
     31 pp.

Pickford, R.  1960.  Survival,  Fecundity and Population Growth of Melanoplus
      b-ilituratus (Wlk.)  (Orthoptera:Acrididae)  in Relation to Date of
      Hatching.  Can. Entomol., 92:1-10.

Pickford, R.,  and R. L. Randell.  1969.   A Nondiapause Strain of the Migratory
     Grasshopper Melanoplus  sanguinipes  (OrthopterarAcrididae).   Can. Entomol.,
     101:394-396.

Smith, D. S.  1966.  Fecundity and  Oviposition in the Grasshoppers Melanoplus
     sangu-inipes (F.) and Melanoplus b-Lvittatus  (Say).  Can.  Entomol.,
     98:617-621.

Stinner, R. E., J.  W. Jones,  C.  Tuttle,  and R. E. Caron.   1977.   Population
     Mortality and Cyclicity as  Affected by Intraspecific Competition.   Can.
     Entomol., 109:879-890.

Taylor, F.  19.80.  Timing in the Life History of Insects. II. Magnitude and
     Hedging Factors.  Ecology.   (In press.)

Weedon, F. R., A. Hartzell,  and  C.  Setterstrom.   1939.   Effects  on Animals
     of Prolonged Exposure to Sulfur Dioxide.   Contrib.  Boyce Thompson
     Inst., 10:281-324.
                                     184

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              POTENTIALLY USEFUL BIOINDICATORS AND BIOMONITORS
                     OF COAL-FIRED POWER PLANT EMISSIONS
                                  SECTION 18

                      OBSERVATIONS ON TWO LICHEN SPECIES
                          IN THE COLSTRIP AREA, 1979

                                S.  Evers?nan
                                  ABSTRACT

                There was a significant increase in sulfur content
            (p<0.05, linear regression ANOVA) in Usnea hirta (L.)
            Wigg.  samples in 1979 and 1977 as distance from
            Colstrip decreased.  Other observations on U.  hirta
            and Parmelia ohlorochroa Tayl. — respiration rates,
            chlorophyll content, percentage of plasmolyzed algal
            cells, rate of photosynthesis — had no significant
            linear or logarithmic relationship (p> 0.05, linear
            and logarithmic regression) to distance from Colstrip.
                                 INTRODUCTION

     Lichens are used throughout the world as bioindicators of air quality
 (Ferry, et al.,  1973; Hawksworth, 1975-1978; Hawksworth and Henderson, 1978,
 1979; Henderson, 1979, 1980).  Two primary techniques have been used in iden-
 tifying and delineating polluted areas: mapping lichen communities near urban
 and industrial areas, and observing specimens transplanted into polluted areas.
 Symptoms induced by pollutants in the field are compared with symptoms in
 laboratory-treated specimens.

     The Colstrip lichen study used a slightly different approach since (1)
 the study began before a pollution source was present and  (2) epiphytic
 lichens are sparse in the Colstrip area.  Two native lichen species  (Usnea
 hir>ta (L.) Wigg, an epiphyte on ponderosa pine, and Parme'i'ia chloTOc'hToa,
 a soil lichen) were observed over a period of years at varying distances and
 directions from the Colstrip coal-fired power plants 1 and 2.  The plants
began operation in September, 1975 and June, 1976, respectively.  Observations
of anatomical and physiological states were compared with  specimens  treated
with S02 in a field fumigation system in Powder River County  (Eversman, 1978,
 1979) 100 km southeast of Colstrip.   This report summarizes observations in
 1979, and compares 1979 results with those of previous years.

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                            MATERIALS AND METHODS

     Usnea hirta samples were collected from 19 ponderosa pine sites 1-70
km from Colstrip (Figure 18.1, Table 18.1).  Monitoring sites within 10 km
of Colstrip support lichen communities only on north and east-facing trunk
bases, so ponderosa pine branches containing U. h-ivta were transplanted
to sites P1-P9 and P17-P19 in September 1975 or April 1976.  All observations
1976-1979 were from these transplanted specimens.  Source of transplants
was Site P10, an east-facing slope 51 km southeast of Colstrip.  All sites
in Custer National Forest, P10-P16, and site P8 on the Northern Cheyenne
Indian Reservation have sufficient native population to use.  Sites P8,
P15, and P16 received transplants for observation of effects of transplant-
ing.  Native P. chloTOchTOa was  collected  from four  grassland  sites
near EPA exclosures (G1-G4), three other sites near ponderosa pine sites
(P3, P4, P18),  and the control grassland site  (G7) .

     Samples were washed with distilled water and stored in air-dry conditions
in the dark at room temperature for no more than  3 weeks  before  laborato-
ry observations.  Respiration rates were determined manometrically for
250 mg samples at 20°C in saturated condition  in the dark.

     Chlorophyll extracts were made in two ways.   (1) 300-mg samples were
extracted with 10 ml boiling methanol, filtered,  returned to 10 ml levels,
then read at 665 run on a Beckman DU spectrophotometer.  (2) Total pigment
and percentages of chlorophyll and phaeophytin were obtained using the
chromatography methods and formulas of Brown and Hooker (1977) .-  This was
an attempt to decrease chlorophyll degradation to phaeophytin by lichen acids.

     Plasmolysis of algal cells was determined by making wet mounts of
thallus tips, then recording the number of yellow, plasmolyzed algal cells
out of 100 cells on each of three slides (300 cells per sample  were
counted)-  Handling of specimens in this way also allowed for close ob-
servation of color and integrity of thallus.   (S02~exposed lichens became
crumbly and yellow; untreated specimens were firm and green.)

     Sulfur contents were determined by the Montana State University Soil
Testing Laboratory, using a dry ash and turbidometric procedure (pers.
comm.).

     Photosynthesis rates were determined by drying samples to  50 percent of
saturated weight,  as determined by drying curves, then placing  them in
flasks in a Gilson respirometer at 10°C in light for 1 hour.  Atmosphere
samples (10 ml) were removed from the flasks with syringes, and injected
into an infrared gas analyzer to determine amount of C02 consumed.  Controls
were respirometer flasks under the same temperature and light conditions,
with no lichen samples.

     Statistical analysis was through the Montana State University Statistical
Center.  Programs used were multiple regression;  one-way analysis of
variance;  Newman-Keuls Q, comparison of means; and log transformations
(Lund, 1980).
                                     186

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                      Northern Cheyenne
                          Reservation
Figure 18 .1.
Map showing lichen  collection sites.  P1-P16 are,
ponderosa pine  sites with Usnea lii-vta; G1-G7 are
grassland where Papmelia chloroehroa was collected.
Sites P8, P15,  and  P16  have both native and trans-
planted U. hirta.   Site P7 has two buttes.  U.  hirta
was collected from  the  top and bottom of a hill at
P14.  P10* = U. hirta transplant source.  TC =
Taylor Creek fumigation sites (ZAPS).
                               187

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Table 18.1.  LOCATIONS AND DESCRIPTIONS OF LICHEN COLLECTION SITES.
             ROSEBUD,  POWDER RIVER, AND BIG HORN COUNTIES, MONTANA;
             1975-1979
Number
Name
Distance, Direction from
Colstrip, Exposure	
Description
  PI    Sarpy Creek
  P2    Castle Rock
  P3    Kluver NE1
  P4    Kluver El
  P5    D. McRae
  P6    Kluver West trees
  P7    Diamond Buttes
  P8    Morning Star View,
        N. Cheyenne Res.
  P9 A  Kluver, near P3
  P10   East Otter Creek
        (transplant source)
  Pll   SEAM 1
  P12   SEAM 2
  P13   Home Creek Butte
  P14   Three Mile Butte
  P15   Ft. Howes
  P16   Poker Jim Butte
  PI 7   BNW//1
  PI 8   BNW//2
  P19   BNW//3
                 48 km Wl ENE exposure
                 16 km W; E
                  7 km ENE; SW
                  5 km E; W
                  7 km S; NNW
                 10 km SE; NW
                 20, 21 km NE; SW

                 26 km SSE; N
                  7 km NE; SW
                 51 km SE; ESE

                 45 km SE; NW
                 45 km SE; NW
                 55 km SE; NW
                 58 km SE; NW
                 70 km SSE; N
                 66 km SSE; NW
                  1 km S; N
                  2 km SE; N
                  1 km NW; SE
                        T2N, R37E, Sec. 36  (BH)
                        TIN, R41E, Sec. 36  (R)
                        T2N, R42E, Sec. 16   "
                        T2N, R42E, Sec. 29   "
                        TIN, R42E, Sec. 36   "
                        TIN, R42E, Sec.  2   "
                        .T2N, R43E, Sec. 22   "

                        T2S, R41E, Sec. 12
                        T2N, R42E, Sec. 16   "
                        T2S, R46E, Sec. 24  (PR)

                        T2S, R46E, Sec. 22   "
                        T2S, R46E, Sec. 22   "
                        T2S, R46E, Sec.  4   "
                        T4S, R47E, Sec. 10   "
                        T6S, R45E, Sec. 19   "
                        T6S, R44E, Sec. 17  (R)
                        T2N, R41E, Sec. 34   "
                        TIN, R41E, Sec.  3   "
                        T2N, R41E, Sec. 28   "
Gl
62
G3
G4
G5
G6
G7

Hay Coulee
McRae Knolls
Kluver West
Kluver North
Kluver East
Abandoned
Field, Taylor
Creek
11
km
SE
TIN,
R42E.
Sec.
28
(R)
Site abandoned "
12
5
21

98

km
km
km

km

SE
E
SE

SE

TIN,
TIN,
TIN,

T7S,

R42E,
R43E,
R43E,

R47E,

Sec.
Sec.
Sec,

Sec.

2
6
15

3

"
ii
"

(PR)

  *
   BH = Big Horn County; R = Rosebud County; PR = Powder River County
                                    188

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                           RESULTS AND DISCUSSION
Respiration Rates

    Observations from the field 862 fumigation sites  (ZAPS plots,
Eversman,  1978,  1979) indicated  that  respiration, rates of the lichens
could be expected to rise when samples were slightly  stressed and to  fall
significantly when subjected to continuous higher S02  stress.  Therefore,
either of these responses was watched for, particularly in samples within
a few km of Colstrip.

    Variation in respiration rates of U. hirta among  sites was significant
in 1979  (ANOVA, P<0.05), but was generally not related to distance from
Colstrip with one possible exception  (Figure 18.2).   U.  hivta transplanted
in 1976 to one of the sites 1 km from the Colstrip power plant (BNW//1) had
a significantly elevated respiration rate July, 1979  (ANOVA, P<0.05).  The
same phenomenon was observed at this site in September, 1977, and at  site
P18 (BNW//2, 2 km from the power plant) September, 1977 and September, 1979.
It appears that these two sites may be affected by the power plants.
     1000
  Q  800
  UJ
  CO
  z
  8  600
   M
  O
        f
         1
                                                                 =0.0001
10       20       30      40       50
         KILOMETERS  FROM  COLSTRIP
                                                          60
                                                    70
 Figure 18.2.
Linear regression of respiration rate of Usnea hirta,
July, 1979, with distance from Colstrip.  Each point
represents the mean of three to six samples.  Regression
line was computed using all readings comprising means.
Distance from Colstrip was not significant (P>.05,
linear and log transformation), although point with
* (Site BNW#1, 1 km from Colstrip) was significantly
higher (P<.01, ANOVA) than other sites.
                                     189

-------
     Regression lines comparing 1976-1979 (July respiration rates only)
are presented in Figure 18.3.  In 1977 and 1978, respiration rates showed
a significant linear relationship to distance from Colstrip (regression
analysis of variance P<0.05, both linear and with log transformation),
however, since the slopes of the lines are opposite, the meaning of this
relationship is unclear.  In 1979, when impact would be expected to have
been greater than in 1977 or 1978, the relation between respiration rates
and distance was not significant  (P<0.05, linear regression and log trans-
formation, with analysis of variance).  Sample size was greatest in 1979;
sample sizes may account for some differences.

     All analyses of respiration rates of P. chloTOchroa gave results that
were not significant; sites were not significantly different from each other
(ANOVA) and respiration rates were not related to distance from Colstrip (re-
gression) . According to ZAPS experiments in 1976, P. chlopochroa was almost
as sensitive to S02 as U. hirta when they were placed side by side about
50 cm above the ground (Eversman, 1978, 1979).  It could be that S02 was
not reaching ground level at the grassland sites, either because it is being
filtered out by grasses and forbs above ground level, or because the plume
from Colstrip was above even grass and forb level at the grassland sites.
     1000
   o
   UJ
      80°
   g  600

    CM
   O
/I978:
                                                                0.02
         1
"1979: r2= 0.02

^1977: r2 = 0.30

M976: r2=0.06
                10      20      30      40      50
                         KILOMETERS  FROM COLSTRIP
60
70
 Figure 18.3.   Linear regressions of U.  hirta respiration rates, 1976-1979,
               month of July only, with distance from Colstrip.  Distances
               were not significant in 1979, but were significant in 1978
               and 1977 (P<0.05,  regression analysis of  variance).   All
               recorded respiration readings during July of each year
               were used for regression computations.  Sample size was
               greatest in 1979 (100 data points) vs. 80 in 1978, 26
               in 1977, and 35 in 1976.   Variation in sample size may
               account for some of the differences.
                                     190

-------
Sulfur Content

    The MSU Soil Testing Laboratory determined percentage of sulfur content
of lichen samples in 1975, 1977 and 1979.  During these years, the laboratory
changed their analysis methods so comparisons between years are invalid
until intercalibrations are available.  Within-year comparisons are possible
(Figure 18.4).  In 1979, U. hirta from the two closest sites to the Colstrip
plant had higher sulfate content than samples from other sites, but dif-
ferences were not significant (ANOVA, Newman-Keuls Q test).  However, sulfate
content of U. hi-rta was related linearly to distance from Colstrip in 1979
(regression analysis of variance, P<.05).

    In 1977, with seven sites sampled for sulfur content (P1-P6, P10-P13),
there was also a significant linear relationship between distance from
Colstrip and sulfur content of U. hirta tissue (r2 = 0.18), P<.05, linear
regression analysis of variance).  In 1975, before power plant operations
began, no linear relationship existed.  Usnea hirta samples seemed to be
accumulating more sulfur in the Colstrip vicinity than in sites farther
away (in Custer National Forest).
  (7)

  2  0.15
     0.10
     0.05
  CO

  3*
                                                             <0.05
                  10       20      30       40      50
                           KILOMETERS FROM  COLSTRIP
                                                           60
70
Figure 18 .4.
              Regression of percentage sulfur (as sulfate) of U. h-ir>ta
              samples, 1979.  Each point is the mean of  three  to  12  samples.
              Regression was computed using all readings comprising
              means.  Increased sulfur content was linearly related
              to distance from Colstrip (negative slope, P<.05, re-
              gression analysis of variance).
                                    191

-------
    Parmelia chlovochvoa samples all had a sulfate content between 0.06
and 0.08 percent in 1979,  regardless of  location.  There were no significant dif-
ferences among sites and there was no linear relationship between sulfur
(as sulfate) content and distance from Colstrip in 1975, 1977, or 1979.

Plasmolysis of Algal Cells

    Counting plasmolyzed algal cells gave an immediate impression of total
thallus health and integrity,  as well as a quantitative measure of
presumably viable photosynthesizing algal cells (Figure 18.5).  It is
perhaps a less objective method than chlorophyll content determination or
apparent photosynthetic rate,  but it does not consume much sample material
nor does it require careful manipulation of temperature, light conditions
and water content.
              -    75|
              a.
              o
              x
              o
  UJ
  o
  cc
  UJ
  0.
CO i
ujT
I CT
L_ *

£ ^
guj
" ^
              a.
              13
                   50
                   25
                 200
            UJ
              8 -200
                -400
                                        -4-
                            25       50     75      100
                       PER CENT  PLASMOLYZED  ALGAL CELLS
             Figure 18.5. Linear regressions of plasmolysis with
                          percentage chlorophyll (acetone wash
                          technique), and plasmolysis with net
                          photosynthesis of U. hirta.   Both re-
                          lations were highly significant  (P<0.01,
                          regression analysis of variance). Data
                          from ZAPS samples (points without
                          circles)  were used in computing the
                          regressions.
                                     192

-------
     Regression lines of plasmolyzed algal cells of U. hirta versus distance
from Colstrip had negative slopes in both 1979 and 1978, but relationships
were not significant (Figure 18.6.).

     Plasmolysis of algal cells in P. chloTOchvoa was not related to
distance from Colstrip, nor were there significant differences in mean
plasmolysis among sites in 1979 (ANOVA) .
CO
«
o
5
to
     40
     30
   <
   _l
   <
     20
   UJ
   o
      10
                                                        1978: r2 =0.31
               10
       Figure 18.6.
                    20      30      40      50
                     KILOMETERS FROM  COLSTRIP
60
70
                  Linear regression of percentage of algal plasmolysis
                  of U. h'lTta with distance from Colstrip.  Points re-
                  present means of three to nine samples collected during
                  1979.  Regression lines were computed using  all data points
                  comprising means.  Plasmolysis was not significantly
                  related to distance from Colstrip in either 1978 or
                  1979  (regression analysis of variance).
Chlorophyll Content
    Until September, 1979, chlorophyll content of lichen samples was
determined by a simple extraction in which lichen materials were boiled
in methanol for a few minutes, filtered, brought back up to 10 ml with
methanol, then read turbidometrically in a Beckman DU spectrophotometer.
Several wavelengths were read, but results were reported as relative
absorbance at 665 nm.  This method actually included chlorophylls, plus
phaeophytin and any methanol-soluble materials.

    It was suggested that the presence of lichen acids destroys chlorophyll,
removing magnesium and forming phaeophytin, thus giving distorted readings
on effects of S02 on chlorophyll (Brown and Hooker, 1977; Nash, pers. comm.)
                                      193

-------
Successive washes in acetone would remove the acids and cause less degrada-
tion of chlorophyll due to acid presence.  The biggest advantage I found of
successive washes in acetone was to allow better separation of pigments
(chlorophyll and phaeophytins) during chromatography, leading to ability to
quantify amounts of each pigment present.  The acetone washes did not com-
pletely remove acids, as detected by addition of paraphenylenediamine
to the last wash, nor was there any apparent beneficial effect on chlorophyll
degradation.

    The two methods gave similar gross estimates of effect of SC>2 on
chlorophyll content Cas judged by ZAPS samples).  There were no significant
relations between distance from Colstrip and percentage of chlorophyll in
extracts (Figure 18.7), or between distance and relative absorbance of
methanol extracts (Figure 18.8).
      80
    i
    a.
    o
    g 60
    _i
    i
    o
    UJ
    o
    cc
    UJ
    0.
      40
       20
                                                      r"=0.04
                                                      P> 0.05
                10      20      30      40      50
                         KILOMETERS  FROM COLSTRIP
                                    60
70
      .Figure 18.7.
Regression of percentage of chlorophyll in pigment
extracts of U. hirta with distance from Colstrip.
Points are means of three samples.  Regression line
was computed using all observations during July,
1979.  This method of chlorophyll extraction (ace-
tone washes, chromatography) gave results similar
to methanol extraction method (Figure 18.8).
                                     194

-------
  in  1.00
  (0
  CO
  o
  a:  0.80
  i-
  X
  UJ
  I
  o
  UJ

  H
UJ
GC
     0.60
  UJ
  o  0.40
CD
0.05, regression
                 analysis of variance).
                                 CONCLUSIONS

   The only measured parameter that showed significant relationship  (P<0.05,
regression analysis of variance) to distance from Colstrip was sulfur content
of Usnea h-irta in 1977 and 1979.  Its significantly higher level in  the
immediate Colstrip vicinity as compared with previous years and with Custer
National Forest sites indicated some power plant effects but still very  slight
at this time.  Samples collected from all sites appeared "normally"  healthy
and appropriately green in 1979 as in earlier years.  Any possible impact
on lichens has been very slight to date, as was expected because of  reported
low concentrations of S02.» ca- 0.10-0.34 pphm monthly averages, at electronic
monitoring stations (Ludwick, e~t al. , 1980) .

   At the end of the 1979 field season, new fresh material was trans-
planted onto many sites (P2-P7, P18, P19) in anticipation of possible
future lichen biomonitoring in the Colstrip area as power plant construction
in the entire study area increases.
                                     195

-------
Value of Lichens as Bioindicators or Biomonitors

     Lichens are not an economically important plant in eastern Montana
ponderosa pine and grassland communities; their ecological importance is
probably not fully understood.  Their role in invertebrate animal communi-
ties may be important, and there are many anecdotal incidents of deer
browsing on epiphytic lichens during winters.

     The ubiquitous use of lichens as air quality indicators in
European countries, Canada and Japan must be considered.  In these
countries where sulfur oxides and acid rains are prevalent, conditions of
lichens and lichen communities are carefully documented.

     Perhaps the line of reasoning is this.  Lichens are green plants,
therefore they have the same basic photosynthetic enzymes and chemical
pathways that higher plants have.  In fact, most of the details of plant
photosynthesis have been elucidated using ChloTella, a green algal very
similar to Trebouxia,  a major green algal component of lichens (including
U. hirta and P.  Ghlorochroa).

     Lichens have some anatomical and physiological differences that
appear to make them more sensitive than most vascular plants, including:
1) Absorbance of water, nutrients, and gases, directly from the atmosphere
with no soil and/or substrate filtering such as that occurring with
vascular plants.  2) Absence of stomata and protective waxy cuticle on
outer surfaces to prevent absorption of materials.   If the lichen thallus
is moist and if pollutants are present, they will probably be absorbed by
the lichen.  3)  Absence of deciduous parts; materials accumulate in-
definitely.  4)  No dormant season of the year; their activity depends on
available moisture, including dew and melting snow, which means they can
accumulate materials throughout the year, not just during a growing season.
5)  The symbiotic system, a balance between the alga and the fungus, may
be more delicate than the conventional tissue system of vascular plants.
If the processes are being impaired in lichens it should serve as a
warning that increasing levels of pollutants will probably cause the same
problem in economically important vascular plants when their protective
mechanisms have been overcome.

     Lichens are an inexpensive bioindicator of air quality, and as such
it seems reasonable to include their use in the monitoring of air quality.
                                REFERENCES

Brown,  D.  H.  and  T,  N.  Hooker.   1977,   The  Significance  of  Acidic  Lichen
     Substances  in the  Estimation  of  Chlorophyll  and  Phaeophytin in Lichens,
     NewPhytol.,  78:617-624.

Eversman,  S.   1978.   Effects  of Low-Level  S02  on Usnae  hirta  and  Parmelia
     ahlorochroa,   Bryologist,  81  (3);367-377.
                                    196

-------
Eversman, S.  1979.   Effects of Low-Level S02 on Two Native Lichen Species.
     In:  E. M. Preston and T. Gullett, eds.   The Bioenvironmental Impact of
     a Coal-Fired Power Plant, 4th Interim Report.  EPA-600/3-79-044.  U.S.
     Environmental Protection Agency.  Corvallis, Oregon,  pp. 642-672.

Ferry, B. W., M. S. Baddeley, and D. L. Hawksworth.  1973.  Air Pollution
     and Lichens.  University of Toronto Press.

Hawksworth, D. L.  1975.  Literature on Air Pollution and Lichens II.
     Lichenologist, 7(1):62-66.

Hawksworth, D. L.  1975.  Literature on Air Pollution and Lichens III.
     Lichenologist, 7(2):173-177 -

Hawksworth, D. L.  1976.  Literature on Air Pollution and Lichens IV.
     Lichenologist, 8(1):87-91.

Hawksworth, D. L.  1976.  Literature on Air Pollution and Lichens V.
     Lichenologist, 8(2):179-182.

Hawksworth, D. L.  1977.  Literature on Air Pollution and Lichens VI.
     Lichenologist, 9(1):77-82.

Hawksworth, D. L.  1977.  Literature on Air Pollution and Lichens VII.
     Lichenologist, 9(2):147-152.

Hawksworth, D. L.  1978.  Literature on Air Pollution and Lichens VIII.
     Lichenologist, 10(1):95-100.

Hawksworth, D. L. and A. Henderson.  1978.  Literature on Air Pollution
     and Lichens IX.  Lichenologist, 10(2):227-230.

Hawksworth, D. L. and A. Henderson.  1979.  Literature on Air Pollution and
     Lichens X.  Lichenologist, 11(1):91-96.

Henderson, A.  1979.  Literature on Air Pollution and Lichens XI.
     Lichenologist, 11(2):313-319.

Henderson, A.  1980.  Literature on Air Pollution and Lichens XII.
     Lichenologist, 12(1);145-148.

Ludwick, J. D., D. B. Weber, K. B. Olsen and S. R. Garcia.  1980.  Air
     Quality Measurements in the Coal-Fired Power Plant Environment of Col-
     strip, Montana.  In: E. M. Preston and D. W. O'Guinn, eds.  The Bioenvi-
     ronmental Impact of a Coal-Fired Power Plant, 5th Interim Report.  EPA-
     600/3-80-052.  U.S. Environmental Protection Agency, Corvallis,  Oregon.
     (In Press) pp. 1-19.

Lund, R. E.  1980.  A User's Guide to MSUSTAT:  An Interactive Statistical
     Analysis Package.   Technical Report.  The Statistical Center, Department
     of Mathematical Sciences, Montana State University, Bozeman.  74 pp.
                                      197

-------
                                SECTION 19

                  EFFECTS OF LOW-LEVEL S02 ON TWO NATIVE
                  LICHEN SPECIES: 1979 ZAPS OBSERVATIONS
                           AND PROJECT SUMMARY

                               S. Eversman

                                 ABSTRACT

               Significant reduction in respiration rate
           occurred in Usnea hi-vta (L.) Wigg. after about 100
           days in a fumigation plot at 2-3 pphm. S02.  At this
           same S02 level, significant reductions in pigment
           content and increases in plasmolyzed algal cells         '
           occurred within 90 days.  At about 5 pphm S02, there
           were significant increases in plasmolyzed algal cells
           within 60 days, decrease in respiration rates within
           60 days, and decrease in pigment content within 90
           days.  Responses of Parmel-ia ohloTOohfoa Tayl. col-
           lected from soil surfaces in the same plots were
           slight and generally insignificant.


                                INTRODUCTION

     The primary  objective  of  this  study was to  establish S02  dose-response
curves for two  native  lichen  species,  Usnea hivta  (L.) Wigg. and Parmelia
ohloTOchToa Tayl.;  i.e.,  to establish  anatomical and physiological  responses
of the lichens  to  given dosages  of  S02 in  the  ZAPS  fumigation  plots.
Laboratory tests  of many  researchers have  established  responses  to  large
doses of S02 in short  periods  of  time  (LeBlanc and  Rao,  1975).   I have
attempted to determine responses  of  U.  hirta and P. chloTookpoa  to  the various
S02 doses of the  ZAPS  plots.

                           MATERIALS  AND  METHODS

     Usnea hirta  samples  were  transplanted to  four  posts in ZAPS plots A,  B,
and C in June,  1979 (the  northwestern  post in  each  plot  was not  used)  by
moving entire ponderosa pine  branches  containing lichen  growth from the
East Otter Creek site  in  Custer  National Forest, 30 km NE of Ashland  (site
P10), as in previous  years.  Collections were  made  28, 56, and 90 days after
transplanting.
                                     198

-------
     Plot D (High) was not observed in 1979; in previous years within
30-60 days lichens in plot D showed nearly 100 percent mortality of  algal  cells,
complete thallus bleaching, significantly reduced respiration rates, and
no photosynthesis.  Since findings in the ZAPS sites have been used for
comparisons with possible responses to S02 in the Colstrip power plant
vicinity, the dosages in D plot were unrealistically high.  Observations in
1979 concentrated in plots A/B and C, ZAPS I and II.

     Parmel-La chloTOclrroa samples from a nearby field were placed at the
base of one post per plot (the most northeastern one) and collected only
in September (90 days of treatment)-

     The major moss in the ZAPS plots (Polytrichum piliferum) and two
Cladonia species were collected from each of the plots to check cell
condition.

     Respiration rates were determined manometrically for 250-mg samples at
20  C in saturated condition in the dark.  Chlorophyll extracts were made
in 1979 according to the method of Brown and Hooker (1977) described in
Section 18.  Plasmolysis of algal cells was determined by counting cells in
wet mounts (Section 18).  Sulfur contents were determined by the Montana
State University Soil Testing Laboratory, using a dry ash and turbidometric
procedure (pers. comm.).  Photosynthesis rates were determined in an infra-
red gas analyzer (Section 18).

     Statistical analyses were through the Montana State University
Statistical Center programs: multiple regression; one-way analysis of
variance, and Newman-Keuls Q, comparison of means (Lund, 1980).

                          RESULTS AND DISCUSSION

     This report summarizes 1979 field observations, and compares and
combines results from this year with previous years to establish lichen
responses to low S02 exposures over 5-month periods in a northern plains
grassland.

Respiration Rates

     The pattern of respiration rates of Usnea hirta. established in previous
years was repeated in 1979.  Figure 19.1 shows results after 90 days
of fumigation in 1979, and results in samples after 92 days of fumigation
in 1978 and 96 days in 1976.  Ninety days of treatment were usually not
enough to establish significant differences in Usnea respiration rates
between A and B plots.  Samples from plot C usually had significantly
lower respiration rates than samples from plots A and B after 90 days of
treatment (ANOVA, P<.05).
                                    199

-------
  7  1000
   i.
UJ jf1
IT
  0  750
£ O  500
CL O
LJ  co
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      250
                               •i     I
                                                           1979 (90 days)
                                                         - 1978 (92 days)
                                                           1976 (96 days)
           OPC

   Figure 19.1.
                  IA
ITA
1C
HC
                               IB     HB
                                 SITE
                  Respiration rates of Usnea hirta, 1976, 1978, 1979, ZAPS
                  A, B and C (means of 3-9 samples ± .95 confidence inter-
                  val computed as tQ.05 x standard error).  Results of  90
                  days exposure in 1979 closely duplicated 92 days exposure
                  in 1978.  Respiration rates of Usnea from plot C were
                  consistently significantly lower than samples from A and
                  B by 100-110 days of exposure (ANOVA, P<0.05).
                  OPC = off-plot control, aa. 2 km from ZAPS plots.

   The assumption was made that treatment in each plot was essentially  the
same from year to year.  Individual respiration rate readings for Usnea
were plotted against days for each plot (Figure 19.2).  Relation between
time in ZAPS I A and II A and respiration rate was not significant (re-
gression ANOVA); the relation was significant in plots B and C, ZAPS I
(regression ANOVA, P<0.05).  There was a significant drop in respiration
rate in samples from plot C after 56 days of exposure and after 96 days in
plot B (ANOVA), P<0..05> Newman-Keuls  Q).

   Respiration rates of PaTme1i,a ehlovoehroa on the ground showed no
significant relationship with ZAPS plots though it responded in a manner
similar to Usnea when placed 50 cm above the ground (Eversman,  1978,
1979).   This position effect is discussed in the following sections.   As
stated previously  (Eversman,  1978)  the bacterial populations associated
with Parmelia probably confound true lichen respiration readings.

Sulfur Content

    There were no significant differences in sulfur content among Usnea
samples from the ZAPS sites after 90 days in 1979  (Table 19.1).  While  the
highest individual readings (0.17 percent, 90 days) and means were from ZAPS B
and C, means were not significantly different (ANOVA, P>0.05).
                                    200

-------
      1000
       75°
 UJ
    UJ
    en
 en _
 LU a.
 cr
       500
       25°
  Figure 19.2,
                                                                = 0.45, P<.OI)
                 25
                                    ON
100
ZAPS
125
150
175
         50      75
      DAYS OF  S02
Regression of Usnea respiration rate with days of SC>2 in
ZAPS I.  Individual respiration readings at 0, 27, 28,
42, 56, 84, 90, 92, 96, 110, 119 and 156 days in ZAPS I
plots 1975-1979 were used in computing regression lines.
Samples from plot A were never significantly different
from day 0.  Samples from B were significantly lower
than day 0 after 96 days.  Samples from C were signi-
ficantly lower than day 0 readings after 56 days (ANOVA,
P<.05; Newman-Keuls Q).
    Results in the Colstrip area indicated some significantly higher
sulfur content in Usnea specimens within 2 km of Colstrip (Section 18)
Perhaps the 90 days of exposure in the ZAPS plots were not adequate to
accumulate different sulfur amounts.  Or perhaps as the Usnea samples
became less viable they were unable to metabolically accumulate sulfur
as healthier specimens do.  Gilbert (1969) demonstrated less sulfur
accumulation by killed Usnea samples than by living ones.

    Sulfur contents were not determined for Parmelia samples from the
ZAPS sites.  In previous years differences across plots were not significant.

Plasmolysis of algal cells

    The only analytical method that consistently showed significant differen-
ces in Usnea and Parmelia samples between ZAPS plots A and B 1976-1979  was
counting plasmolyzed algal cells.  Differences became apparent  at 30  days
and were always significant by 60-90 days  (Figure  19.3; ANOVA,  P<0.05).
Results from Parmelia samples taken from the  soil  surface showed less clear
responses; significantly higher plasmolysis rates  generally occurred  only
in plot D after 60 days of exposure (1975, 1976).
                                     201

-------
TABLE 19.1.  SULFUR CONTENT OF USNEA HIRTA,  ZAPS I AND II,  1979 (MEAN
             PERCENTAGE ± ONE STANDARD DEVIATION FOR THREE  SAMPLES)


IA
IIA
IB
I IB
1C
IIC
July
28 days
0.10±0.03
0.09 ±0.01
0.10±0.02
0.12±0.02
0.11 ±0.02
0.11 + 0.02
August
56 days
0.11 + 0.01
0.11 + 0.02
0.11 ± 0.01
0.11 ± 0.02
0.11 ± 0.02
0.10 ± 0.01
September
90 days
0.11 ± 0.01
0.08 ± 0.02
0.13 ± 0.04
0.11 ± 0.06
0.12 + 0.05
0.12 + 0.05
              OPC
              EOC
        0.09 ± 0.02

        0.12 ± 0.02
0.10 ± 0.03
0.09 ± 0.01

0.11 ± 0.01
              *                        t
               OPC = Off-plot control   EOC  =  East  Otter  Creek,  transplant
               source.     ANOVA,  P = 0.72.
  Q
  LJ
  M
      100
       75
  cn_i
  < LJ
  ^°
  °-   50
  LJ
  O
  CC
  LJ
  Q.
       25
              J-

           i__i
                                                    •I  »•
                                            = 1979 (90 days)
                                            = 1978 (92 days)
                                            = 1976 (96 days)
OPC      IA   IEA    IB      HB
                ZAPS PLOTS
                                                    1C  HC
   Figure  19.3.
   Percentage of plasmolyzed algal cells in Usnea h-irta at
   90 days (1979), 92 days (1978) and 96 days (1976 S02
   exposure, ZAPS I and II.  Differences between A, B and
   C are highly significant (ANOVA P<0.01).  Each bar is
   mean ±  .95 confidence interval (computed as to.05 x
   standard error).  OPC = off-plot control.
                                    202

-------
    Figures  19.4  and  19.5  illustrate  relationships  between time in ZAPS I
plots and plasmolysis rates.   Usnea showed  a more significant response than
Pcametiaj however Usnea was about  50  cm above the ground and Parme'L'La was
on the soil  surface.   Sulfation  plate studies (Eversman, 1978;  Preston and
Gullett,  1979)  showed significantly less S02 reaching 5-10 cm above the
ground (with presumably even  less  at  ground level)  than was detected 50-100
cm higher.   Reduced Parmel-ia  responses,  compared  with Usnea,  were assumed to
be partly a  result of lesser  862 levels at  the soil surface.  Parmelia
appeared to  be  slightly less  sensitive than Usnea (Eversman,  1978), and since
it was directly on the soil,  substrate buffering  may have occurred. Parmetia
control samples tended to  exhibit  slightly  increased plasmolysis throughout
the summer,  from  spring to autumn, that perhaps contributed to  the slope
line in Figure  19.5.

   Taylor,  Leininger,  and Hoard  (pers. comm.) observed significant reduction
of lichen cover in the ZAPS plots C and D since 1976.  I collected Polytr-iohum
piliferum (moss) and  two sterile Cladonia (lichen)  species  from all ZAPS
plots in 1979 for  cell observations.   Cladonia plasmolysis means ranged
between 10-14 percent in ZAPS A and B, 15-18 percent in C, and over 30 percent
in ZAPS D.   It seems likely that some S02 effects were felt by lichens on the
soil surface particularly in plots C  and D.

   Moss cells appeared "normal" in all specimens and there were no visible
differences in moss plants among plots.
   CO
   UJ
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   Q
   UJ
   N
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LJ
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       100
        75
        50
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                                                               = 0.26, P<.OI)
                                                                   I, P=0.32)
             20      40      60      80     100     120
                        DAYS OF S02 ON  ZAPS  I
140
160
   Figure  19.4.
              Regressions of percentage plasmolyzed algal cells of U.
              hirta with time on ZAPS I, plots A, B and C.  Individual
              plasmolysis readings from 0 (day of transplanting), 27, 28
              33, 47, 56, 57, 90, 92, 110 and 119 days in ZAPS I plots
              in 1975-1979 were used in computing regression lines.
              Probabilities are from regression analysis of variance.
                                     203

-------
    0
    Ul
    N
    o
    _l LJ
    a. o
    UJ -J
    O
    o:
    LU
    CL
           50
           25
   Figure 19.5,
                   20      40     60      80     100     120     140
                               DAYS  OF  S02 ON ZAPS I
                                                       160
Regressions of percentage plasmolyzed algal cells of P.
chloTOchroa with time in ZAPS I, plots A, B and C.  Samples
were taken from the soil surface.  Individual plasmolysis
readings from 0 (day of transplanting), 33, 47, 60 and 90
days were used in computing regressions.  Probabilities
are from regression analysis of variance.
Photosynthesis

   Usnea samples from plot C,  ZAPS I and II,  had a significantly reduced
photosynthesis rate after 90 days of exposure in 1979.   Again,  there were
no significant differences between Control samples,  samples from plot A and
most of the B samples (Figure  19.6).  However,  one set  of three Usnea samples
from one position in plot B illustrated a common occurrence in  samples from
this exposure plot.  Samples taken from the most southwestern post tended
to show greater response to S02 than did samples taken  elsewhere in plot B.
Samples from plot B, when averaged together,  consistently exhibited the
greater variances in every characteristic measured (respiration rate,
plasmolysis,  etc,), indicating that the various amounts throughout the plot
seemed to be threshold between slight effect  and pronounced.

 Pigment and  chlorophyll  determinations

     Removal  of  all pigment  from  the  lichen samples has been  very  difficult
 using either boiling  methanol  or  acetone.  Therefore,  determinations of
 pigment and  chlorophyll  content  have been relative between Control  and
 S02~treated  samples,  not absolute.   Regardless  of method used,  differences
 in total pigment content between samples  from  plots A  and B  were  usually
 not significant (Figure  19.7a);  variability  in samples from  plot  B  (ZAPS I
 and II)  was  pronounced.   Samples from plot C had  significantly lower total
 pigment amounts (P<0.05, ANOVA)  than samples from A and  Control plots.

     Stressed chlorophyll degrades to phaeophytin, therefore  higher  levels of
 chlorophyll  were expected in healthy specimens and higher levels  of phaeo-
 phytin were  expected  in  stressed specimens.  However,  samples  treated with
 acetone and  chromatographed  (Brown and  Hooker,  1977) showed  no significant
 differences  across treatments  (Figure  19.7b).   Simple  pigment  extract
                                    204

-------
 LU
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       400
200
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      -200
      -400
                                                I
             EOCOPC   IA HA    IB HB
                     Usnea hirta
                               icnc           F  IA  IB ic
                                          Parmelia chlorochroa
 Figure 19.6. Apparent photosynthesis  rate  of  Usnea  hi-rta  and Parmel'ia'
              olorochroa  after  90  days in ZAPS plots,  1979.  Each bar
              is  the mean ±  .95 confidence  interval  (computed as t.os
              x standard  error)  of three  samples.  Rates were deter-
              mined with  an  infrared   gas analyzer at  50  percent saturation.
              Usnea samples  from one position  in  ZAPS  IB and plots  C
              had net respiration.

 procedures  appeared to be somewhat more informative  in this  case than  the
 more complex  chlorophyll/phaeophytin determination methods.

     Parmel-ia  samples  from the ground in plot C had a significantly  higher
total pigment content, and a slightly higher chlorophyll content than
other samples (Figure 19.7).  These results were similar to those obtained
in 1977.   It appeared that presence of low amounts of S02 was stimulating
pigment production.

    When regressions were  computed between  percentage  of plasmolyzed algal
cells and apparent photosynthesis  rate for  Usnea  (Figure 19.8),  the relation-
ship was highly significant  (regression ANOVA,  P< 0.01).  The relation between
plasmolyzed algal cells and  percentage of chlorophyll  (Figure 19.9) was
slightly less significant  (P<0.05).  Counting  plasmolyzed  algal  cells  gave
not only an observation of gross anatomical  appearance, but also an estimate
of amount of chlorophyll and photosynthesis  rates for Usnea.

     Results for Paimeti-a were  less definitive, with no apparent relation
between plasmolysis, chlorophyll content, and  photosynthesis.
                                     205

-------
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-,
-.
-•
        EOC OPCIA HA I BUB 1C HC
          Usnea hirta
  F IA IB 1C
Par me Ha ch/orochroa
EOC OPC IA HA IB UB ic nc
      U. hirta
F IA IB 1C
P. ch/orochroa
     Figure 19.7a.  Total pigment  content  for Usnea and Parmelia after
                    90 days  in  ZAPS  plot 1979.   Underlines indicate
                    samples  not significantly different from each other.
     Figure 19.7b.  Percentage  of  chlorophyll in pigment extracts of
                    Usnea and Parmelia  after 90 days in ZAPS plots,
                    1979.  Underlines indicate no significant differen-
                    ces across  treatment plots.  Bars are means ± .95
                    confidence  interval (t.     x. standard error) for three
                    samples.  EOC  =  East Otter Creek (transplant source).
                    OPC = off-plot control 2 km from ZAPS. F = field,
                    source of Parmelia  transplants.


                                 CONCLUSIONS

     Usnea hirta  consistently exhibited  better-defined responses to fumigation
 than did Parmelia chloroehroa.   There are  two possible reasons: 1) The
 growth  form of Usnea  is bushy  (fruticose)  and its usual position (tufts on
 bark of trees) give more surface area for  exposure to and absorption of
 S02.  Parmelia is leaf-shaped  (foliose) with proportionately less surface
 exposed to air.  2) Parmelia inhabits soil;  Usnea is an epiphyte on ponderosa
 pine.  The elevated position of Usnea may  expose it to more S02 and the
 acidic bark (pH  less  than 5.0)  offers little buffering potential.  Parmelia
 was  exposed to less S02 probably because of  vegetational scrubbing of taller
 plants around it.  Limestone-derived soils in many places offer buffering
 capacity that would decrease S02 effects.  When Parmelia was elevated on
 ponderosa pine branches with Usnea in 1977 ZAPS observations,  it was
 nearly as sensitive as Usnea (Eversman, 1978, 1979).

    LeBlanc and Rao (1975)  suggested that long-range average concentrations
 of S02 above 3 pphm would probably cause acute  injury  to  epiphytes  in the
Sudbury,  Ontario area.  Results from the ZAPS sites, C  (oa.  5  pphm)  and  D
 (ca.  8 pphm,  geometric means) supported this  statement.   Within 60-90 days
                                     206

-------
           400
    UJ
    tr i
    V)
    UJ
    i
    i-
    CO
    o
    H
    O
    I
    a.
           200
 CM
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O
 o»
 £
 • •
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£
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    UJ
    cc
    <
    a.
    a.
         -200
 CM
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r*=   0.76
P < 0.01
F = 39.75
                          25         50        75         100
              PER  CENT  PLASMOLYZED   ALGAL  CELLS
     Figure 19.8.
            Regression between percentage plamolyzed algal
            cells of Usnea hi-rta and apparent photosynthesis
            rate.  Each dot represents the mean of three
            samples from ZAPS plot A, B and C. I and II
            after 90 days, 1979. P and F values are from
            regression analysis of variance.
thalli were bleached and there were significant decreases in vital processes
(photosynthesis, respiration), in pigment content and cell viability,
especially in Usnea h-ipta.

    LeBlanc and Rao also suggested that long-term SC>2 exposure of 0.6  to
3.0 pphm could cause chronic injury to lichens.  After 60 days in plot B
(ca.  2-3 pphm), Usnea had elevated plasmolysis rates, reduced photosynthesis
and pigment contents, erratic respiration rates, and visibly bleached  thalli.
After 90-100 days in plot B, all of these characteristics showed significant
differences when compared with samples from Control  sites and ZAPS plot A.
Depending upon definitions  of "acute" and "chronic",  samples of Usnea and
elevated Pavmelia, always exhibited adverse effects  after two to three
months in B plots.

    ZAPS plot A has been recorded having about  1  pphm S02 average  (geometric
mean)(Preston, pers. comm.).  The longest lichen  testing period was 156 days
                                   207

-------
      100
   x
   a.
   o
   cr
   o
   _i
   x
   o
75
       50
    LJ
    O

    cr  25
    LU
    Q_
                                                    r^=   0.31
                                                    P =  0.03
                                                    F =  5.97
                     25         50        75         100
           PER  CENT  PLASMOLYZED  ALGAL  CELLS

   Figure  19.9.  Regression between percentage plasmolyzed algal cells and
                percentage of chlorophyll  in pigment extracts for Usnea
                hirta.   Each dot represents the mean of three samples from
                ZAPS I and II,  plots A, B  and C after 90 days,  1979.  P and
                F values are from regression analysis of variance.

in 1976;  the shortest was 84 days in 1978.  Within  these time periods, there
were no significant differences between sampling time and the day of trans-
planting.   The  conclusion from plot A is that it would take more than 156
days of constant S02 exposure at that recorded level to cause detectable
adverse effects in Usnea h-Lrta in this climatic regime.

    When Parmel-ia was extensively sampled  from the  soil most detectable
responses  were  from plot D with mostly statistically insignificant responses
from plots B and C.  The. responses that did occur would have been at SC>2
levels less than the monitored amounts since monitoring devices were placed
above ground level where S02 amounts appear to be higher than directly
on the soil surface.

                                REFERENCES

Brown, D.  H. and T. N. Hooker.  1977. The Significance of Acidic Lichen
    Substances  in the Estimation of Chlorophyll and Phaeophytin in Lichens.
    New Phytol, 78:617-624.
                                   208

-------
Eversman, S.  1978.    Effects of Low-Level of SC>2 on Usnea hipta and
             oKtovochToa.  Bryologist, 81 (3):367-377.
Eversman, S.   1979.   Effects of Low-Level S02 on Two Native Lichen Species.
    In: Preston, E. and T. Gullett, eds.  The Bioenvironmental Impact of a
    Coal-fired Power Plant.  4th Interim Report.  EPA-600/3-79-044 .  U.S.
    Environmental Protection Agency, Corvallis, Oregon pp. 642-672,

Gilbert, 0. L.  1969.  The Effect of S02 on Lichens and Bryophytes around
    Newcastle upon Tyne.  Air Pollut. , Proc. Eur. Congr. Influence Air
    Pollution, Plants and Animals, 1st. 1968. pp 237-272.

LeBlanc, F. and D. N. Rao.  1975.  Effects of Pollutants on Lichens and
    Bryophytes.  In: Mudd, J. B. and T. T. Koslowski, eds.  Responses
    of Plants to Air Pollution.  Academic Press, New York. pp. 237-272.

Lund, R. E.  1980.  A User's Guide to MSUSTAT:  An Interactive Statistical
    Analysis Package.  Technical Report.  The Statistical Center, Department
    of Mathematical Sciences, Montana State University, Bozeman. 74 pp.

Preston, E. M. and T. L. Gullett.  1979.  Spatial Variation of Sulfur
    Dioxide Concentrations on ZAPS During the 1977 Field Season.  In:
    Preston, E. and T. Gullett, eds.  The Bioenvironmental Impact of a
    Coal-fired Power Plant.  4th Interim Report.  EPA-600/3-79-Q44 . U.S.
    Environmental Protection Agency, Corvallis, Oregon,  pp. 306-330.
                                     209

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                                 SECTION 20

                     FLUORIDE AND ARSENIC CONCENTRATIONS
                         IN HONEY BEES  NEAR COLSTRIP

                              J.  J.  Bromenshenk
                                  ABSTRACT

                Since the coal-fired power plants were put in oper-
           ation at Colstrip in 1975 and 1976,  fluorides in bee
           tissues have demonstrated significant increases over      %
           baselines at apiaries downwind and within 20 km of the
           plants.  In the fall of 1979,  fluoride levels at sites
           having concentrations significantly  greater than base-
           lines were similar to 1976,  when some levels were more   /
           than twice those observed before the power plants began v
           operation.  Nearly all fluoride levels for early summer
           of 1979 were substantially higher than any observed in
           previous years.  In 1977, high concentrations of fluoride
           were observed in bees at two sites,  one north and one
           south of Colstrip.  In 1979, mean fluoride levels at the
           south site exceeded that of 1977 by  a factor of 1.5, an
           approximate 11 fold increase over baselines.  No bees
           were at the north site in June of 1979.   At sites north-
           east of Colstrip, June/July fluoride concentrations were
           3 to 17 times baselines.  Levels at  one of these sites  _,/
           exceeded reported bee toxicity thresholds.  Although
           fluoride levels varied significantly in 1979, at none of
           the sites did arsenic levels exceed  baselines.
                                INTRODUCTION

     Literature reviews and detailed rationale for selecting honey bees as
biological monitors appeared in the preceeding five interim reports of the
Colstrip project.   Bees serve as bioaccumulators and magnify the levels of
many chemicals in their surroundings making it easier to detect the presence
and distribution of pollutants.  They also provide information about the
potential for transfer of pollutants through food chains, especially to humans
via honey or pollen.  They are manageable social insects that can inhabit
almost any biome,  and they provide an abundance of sampling material (bees,
pollen, honey, and wax).  Because bees are beneficial insects in terms of
                                     210

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products (honey, wax, and pollen) and services (pollination), information
gathered using a bee monitoring system is directly applicable to human welfare.

     Monitoring honey bees should serve as an early warning system of pollutant
accumulation and effects which may harm other organisms or alter ecosystem
structure and/or function.  Hazards to the bees themselves and to the beekeeping
industry may also be discovered.

     I emphasized fluoride in this study because it is a coal combustion emis-
sion, is relatively simple to detect analytically, has low background levels
in flora and fauna of native grasslands, and is toxic to bees.  Although coal-
fired power plants emit substantially more sulfur than fluoride,  my previous
attempts to examine anthropogenic sulfur in honey bees proved unsuccessful.
High background levels of sulfur in bee tissues (presumably in sulfur bonds  of
proteins) tended to mask any detectable incremental increase  (Hillman, 1972).

     Honey bees take up large amounts of arsenic near copper smelters and have
been reported to take up arsenic emitted by coal-fired power plants  (Lillie,
1972).  Colstrip bees have been monitored for any long-term build-up of this
element, but 1975-78 arsenic levels in these bees, with a few exceptions, have
been low.

     Air and water are the media whereby pollutants released by activities
such as the mining and burning of coal at Colstrip may readily reach bees.
Therefore, fluoride concentrations in apiary water supplies and levels of
fluoride and sulfur in the ambient air have been monitored concurrently with
levels in bees and pollen.

                            MATERIALS AND METHODS

     In 1979, honey bees, pollen, water, and air were sampled at 16 apiaries
during late June/early July and again in mid-September.  Many of the colonies
are transported to California each winter for pollination of orchards and
vineyards and are returned to Montana in April and May.  Any food supplies
(pollen and honey) brought from California were likely consumed and replenished
by June.  Therefore, contaminants carried back with the "migrant" colonies
should be dispersed by the June/July sampling unless fluoride is retained in
the beeswax.  Also, several population turnovers should have occurred (brood
cycles are approximately three weeks).  Colonies distant from Colstrip (>40 km)
are not moved out of the region and can be used as additional controls.  Bees
sampled near Colstrip in June/July had collected several boxes (supers) of
surplus "sweet clover" honey.  This provided further evidence that extensive
foraging and nectar gathering had occurred since their return from California.

     The autumn (September) collection was performed before the apiaries were
transported back to California.  The beekeeper moved the colonies from NE 3
and NE 4 to a stockpile location 1 day before they were scheduled to be
sampled.  I found and sampled these before they were shipped, but it was not
clear in all cases which of the marked hives were from which  of the  two bee-
yards.  Therefore, the results for these sites for September, 1979,  are indi-
cated as NE 3/4.
                                     211

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Bees and Pollen

      Each apiary contained seven to 50 colonies; most had 20 to 30 colonies.
A high velocity, battery-powered, acrylic vacuum apparatus was used to obtain
30 gms wet weight of bees (about 300 bees) from the entrance of each of 10
hives (Bromenshenk,  1978).   At each location,  the samples were immediately
frozen and stored in Whirl  Pacs® at -20°C.

     A plastic pick was used to collect pollen from brood chamber combs of 10
colonies at each location.   The pollen samples were stored in plastic vials at
room temperature.  A 100 gm wet weight pooled  sample  (about 1,000 bees) was
obtained at the entrance of every hive in each beeyard to provide a quick
screening method of analyses, to produce an average sample from each location,
and to ensure sufficient quantities of materials for quality assurance tests,
pesticide tests, and other  tests.

Sulfation and Calcium Formate Plates

     Two sulfation and two  calcium formate plates were mounted on posts at the
grassland canopy level (75  cm above the ground) in each apiary in June and
collected in September in order to measure ambient air concentrations of
reactive sulfurs and fluorides.  All of the analyses were complete, but statis-
tical examination of the data for 1978 and 1979 was incomplete at the time of
this report.

Water

     Water was sampled at each apiary, in addition to bees, pollen, and air.
All beeyards were located within a few hundred meters of easily accessible
water in streams or reservoirs.  A minimum of  500 ml of water was obtained at
points where bees were landing to drink.  Samples were collected and stored in
Naglene§ bottles and frozen until analyzed.  Besides creeks and ponds, any
water in livestock watering tanks within 0.5 km of beeyards was also sampled.

Fluoride Analyses

     Before being analyzed for fluoride, whole bees and pollen were oven-dried
at 45°C for seven days and ground in a Wiley-Mill® to pass a 40-mesh screen.
For each sample, 0.5 gm of ground and dried material was placed in a metal
crucible and slurried with distilled water with 0.05 gm of reagent grade
calcium oxide.  The samples were charred under infrared lamps before being
ashed in a muffle furnace at 600°C for at least 6 hours.  The ashed samples
were digested in 2 ml of perchloric acid and subsequently diluted to 100 ml
total volume with Orion Tisab® total ionic strength activity buffer.  Fluoride
determinations were made using an Orion® specific ion probe inserted into the
150 ml beakers containing the dissolved samples which were stirred constantly
during analysis.  Water was analyzed using the Orion probe and 150 ml of equal
parts of water and buffer solution.
                                     212

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Arsenic

     Arsenic determinations were carried out by F. F. Munshower and A. R.
Neuman, Animal and Range Sciences, Montana State University.  One-g samples
were weighed into 125 ml Erlynmeyer flasks and digested in 30 ml of a 3:2
moisture of nitric perchloric acid.  Samples were left overnight and then
heated slowly to solubilize.  The heat was gradually increased to reduce sample
volume to one-half.  The samples were cooled and 10 ml of a 1:1 mixture of
nitric:sulfuric acid added.  Heat was increased until perchlorate fumes evolved
out of the flasks.  Heating continued until dense white sulfate fumes occurred.
Volume was reduced by heating to 5 ml and the samples allowed to cool.  The
cooled samples were transferred to 50 ml volumetric flasks containing 15 ml of
concentrated hydrochloric acid, 10 ml of water, and 1 ml of 1 percent (w/v)
potassium iodide.  Cooling to ambient temperature and allowing the samples to
stand for 1 hour allowed reduction of As+^ to As+3.

     Standards were prepared in 100 ml volumetric flasks which contained 30 ml
hydrochloric acid, 2 ml of potassium iodide, and 5, 15, and 20 mg of arsenic.
These were allowed to stand for 1 hour prior to analyses.  The coefficients
of determination for the results of analyses for arsenic in the standards
approximates 0.997, indicating good recovery of the chemical.

     All determinations were made using an atomic absorption spectrophotometer
connected to an arsine generator.  The analytical procedure consisted of
placing a 20.0 ml aliquot of standard/sample into the reaction flask.   The
sample was purged by bubbling 50 percent N2 through the solution.  Five ml of
5 percent  (w/v) sodium borohydrate was added through the septum while stirring.

Statistics

     Basic parametric statistical tests (mean, standard deviation, standard
error, 95 percent confidence intervals,  correlation,  two-factor ANOVA; Sokal  and
Rohlf, 1969) were carried out for this report.  Statistical tests of data for
1974 through 1978 suggested that fluoride levels in bees may not be normally
distributed (Bromenshenk, 1979, 1980).  Therefore, the 1979 data will be re-
examined via nonparametric  tests such as Kruskal-Wallis and Wilcoxon two
sample tests (Conover, 1971) in order to examine possible differences in the
distributions of fluoride levels in bee populations.   Also, the data obtained
since 1974 indicates standard errors for fluoride and arsenic which are a
constant function of the mean.  Because of this, M. E. Ginevan, biomathematician
and entomologist at Argonne National Laboratories (personal communication, 1980)
recommends logarithmic transformations of the data prior to applying parametric
statistics.  Each of the above approaches will be undertaken, the results of
which will be published in a final report covering the entire 6-year study
period.  It was not possible to complete these exercises for this progress
report.

                                   RESULTS

     Fluoride levels in apiary water supplies are summarized in Appendix 20.1.
Rosebud Creek, which supplies water to 87 percent of  the beeyards near Colstrip,
displayed relatively constant fluoride levels from 1974 through 1979


                                      213

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(0.4-0.6 ppm).   Water from deep wells (NE 10 and E 2) contained more fluoride
(2.0-8.0 ppm)  and a reservoir (S 1)  had the least fluoride (0.1 ppm).  A live-
stock watering tank and a slough formed by overflow from the tank located at
NE 10 has had the highest fluoride levels (2.6-12.7 ppm).  Although bees have
often been observed obtaining water at Rosebud Creek and at the stock tank and
slough at NE 10, bees were not seen at the stock tank at E 2 and appeared to
be using Rosebud Creek as their primary water supply.

     Fluoride levels in pollen obtained from each beeyard are presented in
Table 20.1.  From 1975 through 1978, mean fluoride levels of pollen obtained
from beeyards did not exceed 3.0 ppm (range 1.5-2.9 ppm).  In 1979, 3.0 ppm
was exceeded in 43 percent of all cases (June/July and September) and 57 percent
of the June/July samples; 4.3 ppm at NE 3 in June was the high.  Mean fluoride
in excess of 3.0 ppm was found in two check samples  (3.4 ppm at SE 6 in Septem-
ber, 3.1 ppm at SE 12 in June/July) as well as at sites near Colstrip.

 TABLE 20.1.  PPM FLUORIDE IN POLLEN, 1979
  Site            Date            X          S.D.          S.E.
N 1
NE 1

NE 2

NE 3
NE 4
NE 3/4
E 2

SE 1

S 4

S 5

S 1

SW 2

SW 3

SE 6

SE 12

NE 1C

Sept.
June/July
Sept.
June /July
Sept.
June /July
June /July
Sept.
June /July
Sept,
June /July
Sept.
June /July
Sept.
June /July
Sept.
June /July
Sept.
June /July
Sept.
June /July
Sept.
June /July
Sept.
June /July
Sept.
June /July
Sept.
1.5
1.9
2,9
2.0
1.8
4.3
3.1
3.6
2.7
2.4
3.8
4.0
3.2
3.4
2.5
2.4
3.2
2.7
2.2
2.6
3.2
2.0
2.7
3.4
3.1
1.6
2.8
3.8
0.69
0.56
0.72
0.57
0.69
0.92
1.43
1.04
1.04
0.84
0.39
0.85
1.06
0.75
1.07
0.74
1.13
0.96
0.42
0.91
1.25
0.55
1.01
1.00
0.78
0.24
0.61
0.51
0.23
0.18
0.28
0.18
0.22
0.29
0.54
0.29
0.33
0.26
0.12
0.27
0.35
0.24
0.34
0.23
0.36
0.30
0.13
0.29
0.40
0.17
0.34
0.32
0.25
0.07
0.20
0.16
9
10
10
10
10
10
7
13
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
                                      214

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     Mean content and 95  percent  confidence intervals for fluoride in worker honey
bees collected in mid-summer and autumn of  1979 are presented in Figures 20.1
and 20.2 and Table 20.2.  Figure 20.1 also  presents a map of the major apiary
locations utilized since  1974.  Figure 20.3 presents mean fluoride content and
95% confidence intervals  for samples taken  in autumn of  1975, 1976,  1977, and
1978.

     Mean fluoride levels of pollen collected from each  apiary in June and
September, 1979, were not significantly correlated (r> =  0.20, df 12, P >_ 0.05),
nor did mean fluoride content of bees collected at beeyards in September signi-
ficantly correlate with mean fluoride content of pollen  collected in September
(r = 0.31, df 12, P _> 0.05).  There was a significant, although weak,  corre-
lation between fluoride levels in pollen and bees from each site (mean fluoride)
and from each hive (r = 0.59, df 11, P <_ 0.05; r = 0.3721, df 126, P <_ 0.01)
based on June/July, 1979, sampling results.

     The absolute mean fluoride content of  honey bees sampled in June/July of
1979 at all sites except  NE 10 exceeded that of the previous 2 years
(Figure 20.1).  A livestock watering tank has been a potential source of
fluoride intake by bees at NE 10 since 1974  (Bromenshenk, 1978, 1979,  1980).
It is impossible to make  meaningful comparisons of 1979  to 1976 data for the
July period.  A breakdown of the electric vacuum sampler in 1976 necessitated
taking bees by sweeping them from honeycombs rather than by catching them at
hive entrances.  Tests conducted in September of 1976 indicated that bees
taken from inside hives contained 50 percent less fluoride than bees collected at
entrances (Bromenshenk, 1978).  However, even doubling the levels of fluoride
reported for July of 1976 would still result in a mean of less than  12 ppm for
Colstrip bees at all sites.  Bees collected from 17 sites in 1975 displayed a
mean fluoride content of  8.7 ppm, SE = 0.44, as compared to 27.8 ppm, SE = 8.87,
for  14 sites in  the same  area in 1979.

     Site NE 4 had a mean fluoride content  of 30.9 ppm in early summer of 1979.
A mean of 153.8 ppm fluoride in bees at NE  3 in June was the highest value
observed at any apiary during the 6 years of this project.  Mean values of
53.2 ppm at S 1  in 1979 and 35 ppm in 1977  greatly exceeded the 4.9 ppm  for
1978 and 5.2 ppm for 1975.  In general, fluoride levels  in bees at all of the
sites near Colstrip, but  not at the "check" sites (SE 6  and SE 12), ranked
among the highest observed in this region.

     Although water contributes fluoride to bees at NE 10, water at NE 4, NE  3,
and S 1 is unlikely to be the source of the fluoride  in  bees.  The reservoir
at S 1 typically contains not more than 0.1 ppm fluoride  (1976 through 1979
data), while NE  2 and NE  3 are supplied by  water from Rosebud Creek  (0.4-0.6
ppm), as are most of the  other Colstrip beeyards.

     Bees sampled in September of 1979 most closely resembled those  of 1976,
both in terms of mean fluoride content and  the geographical distribution of
"elevated" levels of fluoride.  The use of  two-factor ANOVA demonstrated
highly significant year and site differences among variances for 1979  versus
1975 levels of fluoride in autumn samples of worker honey bees:

Fs = 12"73 > F-001[1,22]  = 6'73 (y£ars); Fs = 9'20 >  F.001[24,160] =  2'13  (sites)

                                     215

-------
                                            JUNE/JULY   1979
                                              SW-I
                                SW-3
SE-12
Figure 20.1.  Mean fluoride in worker honey bees and 95 percent confidence inter-
            vals, June/July collections  1977, 1978 and 1979.
                 25-i
               g 20^
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               o
                  15-
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                                                      1979
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NE-IO NE-2  E-2   S-5   S-l   SW-I  SW-3  SE-12
  NE-3/4 NE-I  SE-I  S-4  N-l  SW-2  SE-6
Figure 20-2. Mean  fluoride content and 95 percent confidence intervals  of worker
            honey bees collected in autumn,  1979.  Site E  2 was utilized in 1979
            in lieu of SE 2.   It falls within the forage area (flight  range) and
            has the same water supply as SE  2.
                                    216

-------
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           NE-4   NE-2    S-5    SW-I    SW-3   SE-12
               NE-3    SE-2    S-4    SW-2    SE-6
NE-4    NE-2    SE-I     S-4    SW-I    SW-3    SE-12
   NE-3    SE-2    S-5    S-l     SW-2    SE-6
 Figure 20-3.  Mean fluoride content and  95  percent confidence intervals  of worker honey bees collected in
               autumn,  1975, 1976, 1977 and  1978.   Due to occurrences  such as grass fires,  lack of forage,
                and dry ponds, not  all  sites  were utilized over all  years.

-------
TABLE 20.2.   FLUORIDE CONTENT  OF ADULT  WORKER HONEY  BEES,  1979
Site
N 1
NE 1

NE 2

NE 3
NE 4*
NE 3/4

E 2t

SE 1

S 4

S 5

S 1

SW 1

SW 2

SW 3

SE 6

SE 12

GB 3f
NE 10

Date
Sept
June
Sept
June
Sept
June
June
Sept
Sept
June
Sept
June
Sept
June
Sept
June
Sept
June
Sept
June
Sept
June
Sept
June
Sept
June
Sept
June
Sept
Sept
June
Sept
1
10.5
23.0
15.7
18.6
14.2
175.2
32.4
21.3
16.1
22.0
10.8
20.5
16.9
14.8
6.8
14.2
9.6
43.7
11.1
14.1
14.0
10.1
11.0
14.1
12.3
7.1
7.5
11.1
13.0
10.8
97.8
36.3
2
11.0
23.2
15.3
12.7
14.3
171.8
28.8
15.3
16.9
18.1
16.7
24.1
18.7
20.0
10.2
17.3
13.0
63.5
8.0
14.5
14.3
16.2
12.9
14.5
7.9
5.4
7.1
10.8
6.6
8.3
101.3
25.3
3
10.
20.
15.
16.
13.
135.
34.
20.
17.
16.
11.
18.
16.
16.
7.
15.
5.
53.
11.
11.
13.
17.
12.
11.
10.
6.
8.
7.
7.
11.
116.
14.
7
6
6
2
0
5
6
2
2
1
6
6
3
1
7
7
6
8
2
8
3
7
1
8
5
5
3
7
6
8
4
4
4
5.7
21.2
15.2
17.6
16.1
115.9
22.6
17.1
15.9
22.2
11.3
13.2
18.4
15.0
11.0
19.2
11.0
70.0
10.7
13.5
15.0
12.0
13.9
13.5
12.1
8.5
8.5
9.1
7.8
11.7
104.5
14.9
Sample
5
6.1
30.6
19.3
19.9
14.5
137.6
33.4
19.7
15.9
23.0
12.9
16.1
16.6
13.2
6.7
20.2
7.6
39.5
6.8
13.0
13.3
12.8
12.9
13.0
12.3
7.0
7.7
7.3
9.0
12.9
100.2
7.9
Hives (ppm)
6
7.7
28.3
15.3
15.7
16.1
190.9
32.8
14.1
17.4
24.0
13.4
15.0
13.9
20.6
8.0
15.9
7.9
31.7
7.5
16.1
16.5
7.9
10.3
16.1
12.1
7.2
6.9
11.9
9.8
13.2
94.6
33.2
10
15
15
14
19
182
32
17
16
19
13
25
13
15
4
15
-
49
7
12
13
13
11
12
9
6
8
9
15
11
101
32
7
.5
.4
.2
.2
.7
.2
.0
.7
.9
.5
.7
.0
.8
.4
.9
.9

.0
.6
.3
.8
.2
.1
.3
.7
.5
.4
.8
.4
.5
.0
.7
8
5.4
18.7
18.4
16.8
12.4
109.4
-
16.1
18.7
16.9
13.5
15.5
16.8
18.6
7.8
15.3
13.4
78.1
12.7
14.0
12.4
14.5
8.0
14.0
13.2
5.2
5.3
13.1
10.9
13.4
89.1
14.8
9
6.
28.
17.
18.
13.
150.
-
18.
16.
17.
13.
25.
12.
18.
12.
12.
7.
41.
7.
15.
16.
12.
12.
15.
9.
7.
6.
9.
11.
14.
107.
16.
4
4
9
9
4
5

3
5
0
8
7
6
1
8
4
2
5
7
2
4
1
9
2
0
2
6
3
9
8
0
4
10
6.4
25.3
15.2
16.8
11.8
169.2
-
17.8
-
20.5
16.8
19.1
15.2
20.2
13.4
20.8
9.5
61.5
7.3
13.1
17.7
11.9
19.3
13.1
30.6
8.4
8.8
12.3
6.7
13.8
98.7
15.0
Combined
Sample
8.1
23.7
17.7
15.0
16.5
133.2
34.9
-
18.9
19.1
13.1
18.6
16.4
16.1
13.0
14.9
10.8
59.5
10.9
_
18.0
12.2
15.0
15.0
11.7
6.3
10.3
7.0
14.0
14.3
85.4
32.1
X
8.0
23.5
16.3
16.7
14.6
153.8
30.9
-
17.3
19.9
13.4
19.3
15.9
17.2
8.9
16.7
9.4
53.2
9.1
13.8
14.7
12.8
12.4
13.7
13.0
6.9
7.5
10.2
10.0
12.2
85.4
32.1
S.D.
2.3
4.8
1.6
2.2
2.3
28.3
4.1
-
1.8
2.8
2.0
4.4
2.0
2.6
2.8
2.7
2.7
14.8
2.1
1.3
1.7
2.8
2.9
1.3
6.4
1.1
1.1
1.9
3.1
1.8
7.3
9.9
S.E.
0.74
1.50
0.50
0.69
0.73
8.96
1.29
-
0.57
0.88
0.64
1.41
0.64
0.76
0.88
0.85
0.84
4.68
0.66
0.41
0.59
0.89
0.93
0.41
2.02
0.35
0.34
0.30
0.96
0.58
2.31
3.13
95% Confidence
Interval
6
20
J5
15
12
133
27

16
17
11
16
14
15
6
14
7
42
7
12
13
10
10
12
8
6
6
8
7
10
80
39
.4 -
.1 -
.2 -
.2 -
.9 -
.6 -
2 _
	
.5 -
9 —
.9 -
. 1 -
.5 -
.3 -
.9 -
.8 -
.5 -
.6 -
.5 -
.8 -
.4 -
.8 -
.3 -
.8 -
.4 -
.2 -
.7 -
.9 -
.8 -
.9 -
.2 -
.2 -
9.7
26.9
17.4
18.3
16.0
174.1
34.7

18.2
21.9
14.9
22.5
17.4
19.1
10.9
18.6
11.3
63.8
10.6
14.7
15.8
14.8
14.6
14.7
17.6
7.7
8.3
11.6
12.2
13.5
90.6
19.80
* Only seven colonies in beeyard.
t Located north of SE 2, within same forage area.
  Located at Billings, Montana.

-------
Two-factor ANOVA for 1979 versus 1976 levels of fluoride in bees from August/
September revealed highly significant differences in variances among sites but
not years:

Fs = i'11 < F.05[l,23j " 4'28 (^ears)' Fs = U'14 > F.001[20,144] = 2'51  (sites)

Comparing absolute mean fluoride content of bees (95 percent confidence intervals)
for autumn of 1975 through 1979, levels in 1979 and 1976 were generally higher
than in 1975, 1977, and 1978.

     In both 1979 and 1976, fluoride levels were lowest at sites directly south
of Colstrip and at the "checks" distant from Colstrip.  The 1979 mean fluoride
content of bees samples in September exceeded 1975 baselines and equalled or
exceeded levels observed in 1977 and 1978 at sites northeast, east, southeast,
and southwest of Colstrip (Figure 20.3).  The 1979 fluoride levels in bees
collected in September were lower than those of June/July at many Colstrip
sites, although fluoride levels at apiaries southwest of Colstrip and at the
check sites were essentially the same for both the early and late summer periods.

Fluoride Values for Pooled Samples Versus Mean of Separate Samples

     Values for fluoride in pooled samples versus the mean of independent
samples are presented in Figures 20.4 and 20.5.  Figure 20.4 summarizes data
from all sites from 1974 through 1979.  The correlation coefficient (r = 0.99)
indicates a highly significant relationship, P <_ 0.001.  The coefficient of
determination (r2 = 0.98) indicates that only slightly over 2 percent of variation
in fluoride indicated by the mean of independent observations is due to vari-
ation not associated with "fluoride content" as displayed by the pooled samples.

     Figure 20.5 shows cases in which fluoride content was less than 20 ppm.
Here r2 = 0.80 signifies that 80 percent of fluoride variation in the mean of
independent observations is associated with fluoride, as indicated by pooled
samples.  Again, the association is significant; less than 3 percent of obser-
vations would be expected to fall outside the 30 confidence intervals.
Figure 20-5 includes mean values based on as few as four independent colonies.
I recomputed the correlation coefficient and coefficient of determination for
only those values based on eight to 10 observations and obtained values of
T = 0.94, r2 = 0.883.

Arsenic

     The results pf 63 arsenic determinations demonstrated levels equivalent
to those of baseline at all sites during 1979.  The highest recorded value was
0.51 ppm at E 2 in September; the lowest value was 0.13 ppm at SE 12 in
September.  The data indicated somewhat lower values in bee samples ground in
a Wiley Mill® before analysis, compared with the levels in whole bees.  It was
concluded by the chemist performing the analyses that the ground tissues
remained damper than the whole bees after oven-drying.
                                      219

-------
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      (f)
      LU
      _l
      Q.
      \-
      LU
140-
        120-1
        100-
      UJ
      Q_
      UJ
      o
         so
         60
         40
UJ


|  2°
          0
      Q_
      O.
   0    20   40   60   80   100   120
     PPM FLUORIDE (POOLED SAMPLES)
 CO
 LU
 _l
 Q.

 CO
                                                   LU
                                                   Q
                                                   -z.
                                                   LU
                                                   Q.
                                                   LU
                                                   Q
                                                           O
                                                            I
                                                   LU
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   20-

    18-
    16-

    14-

    12-

    10-

    8-

    6-

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    2-
                                                               0
                                                                                     r2 = o.so
                                                                                     n = 9i
                                                          0   2   4  6   8  10  12  14  16  18  20
                                                            PPM  FLUORIDE  (POOLED  SAMPLES)
  Figure 20 .4.
       Comparison of fluoride content of
       worker honey bees as determined by
       pooled samples and by the mean of
       independent observations over a 5
       year period.
Figure 20 .5.
                                                                  Comparison of fluoride content  of
                                                                  worker  honey bees as determined by
                                                                  pooled  samples and by the mean  of
                                                                  independent observations over a
                                                                  5 year  period for values less
                                                                  than 20 ppm.  The circled values
                                                                  were based on four observations.

-------
                                 DISCUSSION

     Fluoride and arsenic are released by coal-fired power plants.  Measured
stack concentrations of Colstrip Unit 2 indicate a level of 2,130 ± 400  (SD)
ppm for fluoride and 221 ± 20 (SD) ppm arsenic (Crecelius et at,, 1978).
Munshower (personal communication, 1978) has detected increased postoperational
arsenic levels in pine needle sheaths from trees near Colstrip.  His analysis
of 1977 bee samples showed arsenic levels in bees from NE 2 were 2 to 3
times higher than baseline and check site levels.  Other investigations have
shown substantially higher fluoride levels in mice and pine foliage from sites
near Colstrip compared to more distant sites (Gordon et al. , 1978, 1979).  My
own studies have repeatedly demonstrated significant postoperational fluoride
changes in bees from apiaries downwind and as far as 20 km from Colstrip
(Bromenshenk, 1976, 1978, 1979,  1980).

     Fluoride in honey bees was  used in this study as a tracer in an attempt
to determine the distribution patterns of the power plant plumes.  The 1979
fluoride data in bees is consistent with previously reported wind patterns
(Van Valin et al. , 1980; Ludwick et al. , 1980; Bromenshenk,  1979).

     Although summer winds are usually westerly during the daytime,  night
surface winds are variable and typically light.  Furthermore, the plumes from
the power plants are affected by the underlying terrain topography being
diverted from the direction of the prevailing winds by as much as 20°.   Plumes
follow valleys and are deflected around higher terrain (Van Valin et al., 1980).
It appears that plumes may be trapped in valleys and then flow southward with
northerly winds mixing at times  to ground levels (Ludwick et al., 1980).
Plumes have been tracked as far as 50 km from Colstrip.  Therefore,  although
several years of wind tower data gathered by the Montana State Department of
Health suggest  that prevailing winds in order of importance are E-SE,  W-NW,
and E-NE, this may be only a crude approximation of plume dispersion patterns.
The data obtained from the sulfation and formate plates which were set out in
1978 and 1979 at each apiary should prove useful in determining whether fluoride
is reaching the apiaries via the air.  Unfortunately, the analytical results
were not returned in time for incorporation into this report.

     As in previous years, the highest fluoride levels in bees in autumn of
1979 were at apiaries located in a "downwind" or easterly direction from        '
Colstrip (NE, SE, E).  Apiaries  directly south and north of Colstrip ancj the
more distant checks exhibited levels essentially identical to baselines.  Also,
as in other years, sites located just west of directly south displayed inter-
mediate levels of fluoride somewhat higher than baselines.  The results from
autumn of 1979, both as regards  levels and the geographic distribution of
fluoride in bees, were similar to those of 1976.

     At all locations including the checks, the June/July fluoride content of
bees was as high or higher than those observed in 1977 and 1978.  A prolific
flowering of yellow sweet clover in June provided plentiful supplies of nectar
and undoubtedly stimulated foraging activity.  This may have contributed to
the generally higher fluoride levels because of more flight activity, greater
probability of contact, more materials brought back to the hives, etc.  However,
                                      221

-------
mean fluoride content of bees obtained at each of two "check" apiaries in 1979
(approximately 40 and 80 km from Colstrip) was lower than that of the bees
from the Colstrip locations.

     Disregarding NE 10, the highest fluoride concentrations for 1979 occurred
at NE 3, NE 4, and S 1 during June and July.  Only once before were levels
greater than 30 ppm observed—at sites N 1 and S 1 in June/July, 1977.  Dumping
mine waste waters into Arnell's Creek (the apiary's water supply) may have
caused high levels of fluoride in bees at N 1 (Bromenshenk, 1980).  No source
of the fluoride at the other sites is known.  It was not in any of the water
supplies sampled.  These fluoride levels are cause for concern.  Levels
observed at NE 3 could poison bees based on literature reports and my own
observations (Bromenshenk, 1980).

     Long-term studies are needed to determine how serious these fluoride
levels in bee systems may be and how the bees are taking up the fluoride.  The
weak correlation of fluoride levels in bees and pollen collected in June/July
suggests the airborne fluoride may be reaching the bees via the food.  However,
one would expect the highest levels to occur in nurse bees or pupae if bioaccu-
mulation is via pollen and in foragers if from nectar.  My previous studies
(Bromenshenk, 1978, 1979, 1980) showed little if any fluoride accumulation in
pupae and hive bees (mainly nurse bees)  and very low levels of fluoride in
floral parts, which provides indirect measure of fluoride in nectar.   It is
possible that the high fluoride concentrations observed in field bees came
about as a result of exposure to airborne contaminants either via penetration
of the cuticle, which seems unlikely, or via the tracheal system.  This is an
attractive hypothesis since food correlations (pollen) are so low, r2 < 14 percent

     However, there are possible explanations for such a weak correlation
between levels in pollen and bees.  P. Tourangeau, who carried out all of the
fluoride analyses, suggested that the levels of fluoride in pollen are near
the lower limits of detectability of the Orion probe, using our present
methods, and the sensitivity may not be good enough in this range to reliably
separate the signal from the noise.  We currently are investigating this
possible source of error.

     There is always the possibility that the fluoride seen in early summer
got into the bee systems before the colonies were set out in the Colstrip area.
However, it is likely that the fluoride accumulation was actually caused by
exposures in Montana.  Any fluoride carried back in colonies exposed at
apiaries in California during the winter should be diluted and "cleaned out"
by June/July for the following reasons:

     1.  Preoperational studies did not detect any fluoride carried back
         from California.

     2.  Except for the brood boxes, none of the equipment is taken to
         California.  Brood cells are lined by bees with a "papery" material
         which effectively isolates the brood from the wax.

     3.  Bees are returned to Montana with marginal food stores which are
         rapidly consumed.

                                      222

-------
     4.   The bees had been at the Colstrip locations since late April and
         early May which is sufficient time for replenishment of stores and
         for several population turnovers.

     5.   All of the sampled colonies had a considerable amount of surplus
         honey in the "honey supers" at the time of collection, indicating
         they had been at the beeyards long enough to build up food reserves.

     6.   Marked hives taken to California and located upon their return
         indicated that the boxes become well mixed and more or less
         randomized while being stockpiled, inspected for disease,  split
         to form new colonies, and transported via truck.

     Also,  one would not expect to see all colonies within a given Colstrip
apiary displaying- similar levels of increased fluoride, &-<3- , NE 3 samples
were all greater than 100 ppm, those of S 1 were all greater than 31 ppm but
less than 70 ppmseta.   Fluoride brought back from California should show up
as a more random pattern—some colonies at a given location displaying high
levels,  others intermediate and some very low—since the colonies at any
Colstrip beeyard probably came from several California beeyards.

     As in all previous years, the fluoride in bees at NE 10 appeared to be
associated with the fluoride in water in a nearby stock tank.  These colonies
were moved farther from the tank and closer to Rosebud Creek in 1979 in an
attempt to change their water supply.  Fluoride levels in these bees was still
high in June/July but for the most part were below 100 ppm.  They declined to
less than 36 ppm by September.  Although high, these levels, especially in
September,  are lower than those observed in individual colonies at this site
during previous years and are below the 120-130 ppm levels, which seem to
"definitely" indicate acute poisoning.  The colonies at this apiary have always
been characterized by a lack of vigor, poor brood laying, and low honey
production.  In 1979, the beekeeper reported that this was one of his best
apiaries, producing more than twice as much honey per colony as in previous
years.  This suggests at least a partial solution to this specific problem and
tends to confirm the assumption that fluoride levels exceeding 100 ppm were
affecting these colonies.  However, the data from 1979 indicate that merely
moving the bees farther from a "contaminated" water supply and closer to a
"clean" water supply does not guarantee that the bees will utilize the
preferred one.

     The fluoride levels in water at sites other than NE 10 were almost
identical to previous levels, and water does not appear to be the source of
the high fluoride levels in the bees during either of the 1979 sample periods.
A stock watering tank about 0.3 km from E 2 contained more fluoride than
Rosebud Creek, which was very close to the apiary.  The fluoride concentration
in bees at E 2 was higher in June/July than in September, but that of the water
was considerably higher in September.  Thus, it is improbable that the stock
tank in this case was a major contributor of fluoride.

     It is possible that fluroide in water may be a contributing factor.  Many
ranchers in the area have complained of wells going bad since the mining
activities began.  Also, mine waste waters apparently have sometimes been

                                      223

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discharged into streams.   However,  most apiaries are located near Rosebud Creek
and relatively distant from other water supplies; fluoride levels in the
Rosebud have remained almost constant since 1974.

     It is becoming apparent that fluoride either via air and/or water is
reaching apiaries near Colstrip and at levels which may pose potential hazards
to bees and beekeeping.   The fluoride data from 1979 raises many questions and
only suggests possible answers.

     Although arsenic appeared at relatively high levels at an apiary northeast
of Colstrip in 1977, this was not observed in 1979.  If arsenic were to sporad-
ically impact the apiaries, longer  term monitoring would be needed to adequately
address potential for buildup of this toxic material.  One might expect to see
correlations between levels of arsenic and fluoride in bees if these materials
are being inserted into their environs by the combustion of coal or by coal-
mining activities.  The one instance of "elevated" arsenic in 1977 was at a
site that over the years has tended to display higher fluoride levels.
According to Crecelius et at.  (1978), 10 times more fluoride than arsenic is
emitted by the power plants.  Thus, it is not surprising that arsenic levels
in bees are low in comparison to fluoride.  In addition, the two contaminants
are dissimilar in physical and chemical aspects which may affect factors such
as dispersion and transport in the  plume, uptake routes into bee systems,
chemical forms encountered, and biochemical/physical chemical interactions.

                                 CONCLUSIONS

     Honey bees collected in 1979 at apiaries within 20 km of Colstrip,
Montana, failed to show any arsenic levels above baselines but continued to
show significant postoperational fluoride changes compared with preoperational
levels.  Unusually high mean fluoride levels in bees, ranging from 2 to 17
times baselines, were found at several beeyards sampled in early summer.  These
levels in bees did not correlate with levels in water supplies.  A significant
correlation (P _< 0.05) was obtained for fluoride in pollen and bees, although
the correlation coefficient was weak (r = 0.37).

     Bees and pollen from a site northeast of Colstrip in June of 1979 had the
highest mean fluoride content (154  and 4.3 ppm, respectively) ever recorded
from southeastern Montana.  According to literature reports and my own obser-
vations, this level indicates poisoning.  Levels greater than 30 ppm were
observed at sites northeast and south of Colstrip during June/July, 1979.
Very high fluoride values were observed in June/July of 1977 at two sites.
One of these was S 1, which in 1979 had 1.5 times the "high level" of 1977 or
53 ppm versus 35 ppm; baselines averaged 5 ppm for this site.

     Fluoride concentration in the  autumn, 1979, collections did not demon-
strate the unusually high levels of the earlier sample period, although mean
fluoride was approximately double that of baselines at sites northeast and
southeast of Colstrip and somewhat  higher than baselines at sites southwest of
Colstrip.  The patterns of fluoride concentration and distribution were very
similar to significant postoperational increases of fluorides in these bee
systems in 1976.  Fluoride concentrations in bees from the "check" sites
approximated baselines,  and levels in September were the same as those in July.

                                      224

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APPENDIX 20.1.  PPM FLUORIDE IN APIARY WATER SUPPLIES, 1979
Dates
June/
July
Sept.
NE 10 NE 4 NE 3 NE 2 NE 1 N 1* E 2t E 2
0.6 0.6 0.6 0.6 0.4 - 2.6 0.6
0.5 0.4 0.6 0.6 - 0.4 6.3 0.6
SE 1 S 5 S 4 S l:j: SW 1 SW 2 SE 3 NE lOt
  June/
   July     0.6       0.6     0.6      0.1    0.4      0.4     0,6      8.3

  Sept.     0.6       0.5     0.6      0.1    0.4      0.6     0,6     10.4
Rosebud
Sites
X
S.D. =
S.E. =
N
Creek
(1977)
0.51
0.03
0.01
10
Rosebud
Sites
X
S.D. =
S.E. =
N
Creek
(1978)
0.55
0.10
0.03
10
Rosebud
Sites
X
S
S
N
Creek
(June/July 1979)
=
.D. =
,E. =
^
0.55
0.09
0.03
11
Rosebud Creek
Sites
X
S.
S.
N
(Sept
_
D. =
E. =
=
. 1979)
0.54
0.08
0.03
10
     *  Arnell's  Creek (a dry creek most of the  summer).
     t  Livestock Watering Tank.
     t  Reservoir.
                                    225

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Regression analyses of the results of fluoride determinations for samples
"pooled" at the time of collection versus the mean fluoride content of four to
10 "individual colonies" revealed significant, P ^ 0.001, correlations.
Pooled samples appear to be adequate and reliable for use in a rapid screening
procedure to locate "hot spots" of pollutant contamination.  Observations of
values for individual hives increases information content but may not be
necessary for an initial monitoring effort.

     The 1979 data raises critical questions, while only suggesting answers.
It is apparent that fluoride is impacting apiaries near Colstrip at levels
which may harm bees and beekeeping.  Whether the fluoride is coming from air
or water or both media is unclear.  Patterns of fluoride in pollen and the
geographical distribution of fluoride buildup with respect to Colstrip and the
prevailing winds suggest airborne fluoride.

                                 REFERENCES

Bromenshenk, J. J.  1976.  Investigations of the Effects of Coal-Fired Power
     Plant Emissions Upon Insects, Report of Progress.  In:  The Bioenviron-
     mental Impact of a Coal-Fired Power Plant, Second Interim Report,
     Colstrip, Montana.  R. A.  Lewis, N.  R.  Glass, and A. S. Lefohn, eds.
     EPA-600/3-76-013, U.S. Environmental Protection Agency, Corvallis,
     Oregon.  pp. 112-129 and 286-312.

Bromenshenk, J. J.  1978.  Investigations of the Impact of Coal-Fired Power
     Plant Emissions Upon Insects.  I.  Entomological Studies in the Vicinity
     of Colstrip, Montana.  II. Entomological Studies at the Zonal Air
     Pollution System.  In:  The Bioenvironmental Impact of a Coal-Fired
     Power Plant, Third Interim Report,  Colstrip, Montana. E. M. Preston and
     R. A. Lewis, eds.  EPA-600/3-78-021, U.S. Environmental Protection Agency,
     Corvallis, Oregon.   pp. 146-312 and 473-507-

Bromenshenk, J. J.  1979.  Honeybees and Other Insects as Indicators of
     Pollution Impact from the Colstrip  Power Plants.  In:  The Bioenviron-
     mental Impact of a Coal-Fired Power Plant, Fourth Interim Report,
     Colstrip, Montana.  E. M.  Preston and T. L. Gullett, eds.  EPA-600/3-79-044,
     U.S. Environmental Protection Agency,  Corvallis, Oregon.  pp. 215-239.

Bromenshenk, J. J.  1980.  Accumulation  and Transfer of Fluoride and Other
     Trace Elements in Honeybees Near the Colstrip Power Plants.  In:  The
     Bioenvironmental Impact of a Coal-Fired Power Plant, Fifth Interim
     Report, Colstrip, Montana. E. M. Preston and D. W. O'Guinn, eds.
     EPA-600/3-80-052, U.S. Environmental Protection Agency, Corvallis, Oregon.
     pp. 72-95.

Conover, W. J.  1971.  Practical Nonparametric Statistics.  John Wiley and
     Sons, New York, New York.  462 pp.
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Crecelius, E. A., L. A. Rancitelli, and S. Garcia.  1978.  Power Plant
     Emissions and Air Quality.  In:  Potential for Gaseous and Heavy Metal
     Contamination from Energy Extraction Processes in the Northern Great
     Plains and the Consequent Uptake and Turnover in Range Ecosystems, ERDA
     Annual Report.  Activity RS-02-03, Ames Laboratory, Iowa State University,
     Ames, Iowa.  pp. 9-33.

Gordon,  C. C.,  P.  C. Tourangeau,  and P. M. Rice.   1978.   Potential for Gaseous
     Contamination from Energy Extraction Processes in the Northern Great
     Plains.   In:   Potential for  Gaseous and Heavy Metal Contamination from
     Energy Extraction Processes  in the Northern Great Plains and the Consequent
     Uptake and Turnover in Range Ecosystems.  ERDA Annual Report, Activity
     RX-02-03,  Ames Laboratory, Iowa State University, Ames, Iowa.  pp. 53-137.

Gordon,  C. C.,  P.  C. Tourangeau,  and P. M. Rice.   1979.   Foliar Pathologies of
     Ponderosa Pine Near Colstrip.   In:  The Bioenvironmental Impact of a
     Coal-Fired Power Plant, Fourth Interim Report, Colstrip, Montana. E. M.
     Preston and T. L. Gullett, eds.  EPA-600/3-79-044,  U.S. Environmental
     Protection Agency, Corvallis,  Oregon,  pp. 141-214.

Hillmann, R.  C.  1972.  Biological Effects of Air Pollution on Insects,
     Emphasizing the Reactions of the Honeybees (Apis mellifera L.) to Sulfur
     Dioxide.   Ph.D. Thesis, The  Pennsylvania State University, University
     Park, Pennsylvania.  159 pp.

Lillie,  R. J.   1972.  Air Pollutants Affecting the Performance of Domestic
     Animals—A Literature Review.   U.S.D.A. Agriculture Handbook No. 380.
     109 pp.

Ludwick, J. D., D. B. Weber, K. B.  Olsen, and S.  R. Garcia.  1980.  Air
     Quality Measurements in the  Coal-Fired Power Plant Environment of Colstrip,
     Montana.   In:  The Bioenvironmental Impact of a Coal-Fired Power Plant,
     Fifth Interim Report, Colstrip, Montana. E.  M. Preston and D. W. O'Guinn,
     eds.  EPA-600/3-80-052, U.S. Environmental Protection Agency, Corvallis,
     Oregon,   pp.  1-19.

Sokal, R. R.  and F. J. Rohlf.  1969.  Biometry.  The Principles and Practice
     of Statistics in Biological Research.  W. H. Freeman and Company,
     San Francisco, California.  776 pp.

Van Valin, C.  C.,  R. F. Pueschel, D. L. Wellman, and G.  M. Williams.   1980.
     Plume and Aerosol Properties Near Colstrip.   In:  The Bioenvironmental
     Impact of a Coal-Fired Power Plant, Fifth Interim Report, Colstrip,
     Montana.  E. M. Preston and D.  W. O'Guinn, eds.  EPA-600/3-80-052, U.S.
     Environmental Protection Agency, Corvallis, Oregon,  pp. 20--48.
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                                  SECTION  21
            BASELINE  HISTOLOGY  OF  SELECTED  ORGANS  OF THE  DEER MOUSE,
             PEROMYSCUS MANICULATUS,  IN  ROSEBUD COUNTY,  MONTANA
                          M.  D.  Kern  and  R.  A.  Lewis
                                   ABSTRACT

                 The  normal  histology of selected  organs of  the
            deer mouse (Peromysous manieulatus)  is  presented.   We
            believe  that  these organs are especially sensitive to
            long-term insults by low  levels  of pollutants such as
            those produced  by coal-fired power plants.  We  also
            suggest  that abnormalities  in their structure due to
            such stress  will be  readily perceived by gross  and
            histological  examination.  The organs include  the  male
            accessory reproductive glands, ovary, uterus,  vagina,
            adrenal  gland,  spleen, liver,  and  kidney.   Descrip-
            tions of  the  testis,  epididymis,  and heart of  the  deer
            mouse appear  in  an  earlier report (Lewis et al..,
            1978).
                                 INTRODUCTION
     This portion of our investigation of the deer mouse (Peromyscus man-
 i-Qulatus  )  provides   quantitative  descriptive  information  concerning  the
normal  histology  (central  tendency   and   variation)   of  selected  organs.
Anatomical  and  histological abnormalities  may provide  useful  indicators  of
long-term pollution impacts.   The organs studied  include the  male  accessory
reproductive glands,  ovary, uterus,  vagina,  adrenal gland, spleen,  liver, and
kidney.   A basic understanding of  these structures will help us  to  assess or
predict  trends  and impacts  of  pollutants  from  coal-fired power  generation
(Lewis et al . ,  1978;  Lewis and  Lewis,  1979).   These data are,  in  any event,
essential to the interpretation of impacts that may occur in the  future.
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                             MATERIALS AND METHODS

     Mice were  trapped in  southeastern Montana and  transported  alive to our
field laboratory (Lewis et> al. ,  1978) where they were sacrificed and dissected
in random rotation.  Organs were immediately placed in 10 percent buffered
neutral formalin or Bouinrs solution.  They were later weighed and examined in
the laboratory, and then dehydrated, embedded in paraffin, and sectioned for
histological study.  Representative sections were stained with haematoxylin
and eosin and evaluated.
Accessory Sexual Glands

     The growth and maintenance of the accessory sexual glands depend directly
on androgen production  by the testis and  in  some  cases characterize a male's
reproductive condition  better than  the  testis  itself  (Ewel, 1972).  Accord-
ingly,  they are  useful  indicators  of  general  reproductive condition,  and
specific androgen  production.

     We examined the vesicular gland, coagulating gland, and ventral prostrate
glands  for  general structure,  size, and  seasonal  changes.  In  addition,  we
used an ocular  micrometer to determine the average  diameter  of  each gland in
section.  We also measured  the  maximum diameter of this fusiform-shaped vesi-
cular gland.  Average tubule diameter is  based on 10 independent measurements1,
of the  width of  each vesicular gland.  Measurements of 10 separate tubules
(or  acini)  were  made  in the  case  of the  ventral  prostrate and coagulating
glands.
     Examination of the  ovary is probably the most  reliable  method of deter-
mining  the reproductive  condition  and  maturity  of  female  deer  mice.   For
example,  mature  females  have ovaries that  contain corpora  lutea  (endocrine
glands  that  develop from  ovulated  follicles), but  immature  animals  do  not.
The  number of  corpora  lutea  in the ovary  is  also  a measure  of fecundity
(number of eggs  ovulated)  and may be used  to  determine the egg production of
mice  (Coutts and Rowlands, 1969).  The number of sets of corpora lutea, number
of  degenerate  (atretic)  follicles,  abundance  and appearance  of interstitial
tissue  (which produces steroidal hormones),  and the number and size of ovarian
follicles  within the  ovary  provide  information  about previous  and  current
reproductive activity.   Since follicular development  is  regulated  by gonado-
trophins produced by  the anterior pituitary gland, ovarian histology can also
be used to assess pituitary function (e.g., Clarke and Kennedy, 1967).

     Fixed ovaries (prior to imbedding)  were examined with a dissecting micro-
scope for grossly visible follicles, corpora hemorrhagica (follicles that have
just ovulated),  and corpora  lutea.   The  following criteria were  used  to dis-
tinguish  among  the three:   1.   Corpora  hemorrhagica.--Small,  punctate  blood
spots  on  the  surface  of the ovary;  2.  Corpora  lutea.--Round  protrusions of
variable  size  (classified as small,  medium,  or  large) on  the  surface of the
ovary;  always  solid  and  curdlike  in  appearance;  3.   Mature  (Graafian)
follicles.--Small  (always!)  round  protrusions  on the surface  of  the ovary;

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hollow, and  in this way  different from  small corpora  lutea  with which they
might  otherwise  be  confused—a  liquid-filled  center   (antrum)   is  visible
through the wall of the follicle.

     Serial  sections  of at  least half of  each  ovary  were examined  for the
number and size of (1)  follicles  at various  stages of development,  (2) corpora
hemorrhagica, (3)  corpora  lutea,  (4) atresias, and (5) scara (corpora albican-
tial).   We also noted  the  amount and functional  state  (based  on histological
considerations) of interstitial tissue.
Uterus and Vagina

     Uterus and vagina  are  two  of the major  regions  of the reproductive duct
of female deer mice.  The vagina is especially useful for assessing the repro-
ductive condition of an animal because there are obvious changes in its struc-
ture  at  various  stages of  the  cycle,  during  pregnancy,  and  during sexual
development.  In  contrast,  changes in  the  structure of the  uterine  horn are
subtle and difficult to interpret.  It is nevertheless very useful for identi-
fying  newly  pregnant   females  or  those whose  reproductive  tracts  contain
embryos (blastocysts) that have not yet implanted.

     We examined  the uterine  horn and vagina for  changes  associated  with the
principal  reproductive  states of  female deer  mice — reproductive  inactivity,
stages of the  cycle,  pregnancy,  parturition  and the  immediately postpartum
state, and  lactation.   We concentrated  on  epithelium, glands  in  the uterine
horn,  contents  and size  of  the  lumen,  and characteristics  of  the connective
tissue (lamina propria)  and  muscle (tunica  muscularis).  In the uterine horn,
we quantified the  height, mitotic activity, and number of  inflammatory cells
within the  endometrial epithelium; the  number of uterine  glands,  their dia-
meter, and  contents; the  vascularity  and width of the  lamina propria and the
degree to which  it was infiltrated with inflammatory  cells;  and the width of
the  tunica  muscularis.   These  characteristics were  measured with an ocular
micrometer or evaluated on a scale of  0 (none present) to 5 (very many or very
high concentrations present).  Averages  are based on at least 10 measurements
of each structure.)
Adrenal Gland

     The  adrenal  gland  of the  deer  mouse, like  that of  mammals generally,
consists  of  two  distinct  and  functionally  independent  glands:  an  inner
medulla which produces catecholamines  (e.g., epinephrine), and an  outer cortex
which produces steroidal  hormones  (e.g.,  corticosterone).  Both parts respond
to  internal  and  external  stressors.   Epinephrine,  for  example,  prepares the
body to  deal with  immediate  emergencies,  increasing  respiratory and cardio-
vascular  activity,  elevating  blood sugar,  and-redirecting  blood flow.   As a
biomonitor, the adrenal  gland  has  the advantage of high sensitivity to exter-
nal stressors.  There is  the  further  advantage that this  gland  responds non-
specifically to stress and therefore integrates all sources.  The  condition of
the adrenal gland thus  provides  a basis not only for evaluating the degree of
stress chronically recently experienced, but also provides information regard-
ing tolerance or potential resilience to additional  insults.

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     Its  involvement  with  reproduction  and  certain  other  activities   (see
below) may  complicate structural  interpretation.   However, knowledge  of its
normal structure in field populations of deer mice is essential to any evalua-
tion of changes  that may occur at sites of coal combustion.

     To assess  adrenal  activity,  we measured the cross-sectional areas of its
major  regions and the lipid  content of the cortex.  We also noted degenerative
and pathological changes.

     To determine  cross-sectional areas  of  regions of  the gland,  we treated
them as a series of concentrically arranged ellipsoids in cross-section.  Four
such  ellipsoids exist  in the  normal  gland.  The  innermost  is  the medulla.
This is surrounded by the  three major regions of the adrenal cortex:  the zona
reticularis  (ZR) ,  zona fasciculata  (ZF) ,  and zona  glomerulosa  (ZG) ,  in that
order.  Accordingly,   the  other  three  ellipsoids  are  combinations  of  (1)
medulla and surrounding  ZF,  (2)  medulla,  ZR,  and  surrounding ZF,  and (3)
medulla, ZR, ZF, and  surrounding ZG.  Because the area of ellipsoid  is TT ab/4,
where  a and b are its major  and minor diameters, respectively, cross-sectional
areas  of each  ellipsoid were readily obtained  from  measurements  made with an
ocular micrometer.   However, it was  necessary to  combine  the ZR  and ZF for
analysis because the  boundary between them was frequently  indistinct.

     Mice that  are  either immature or have never been pregnant sometimes have
additional  cortical  zones with unknown functions  (Howard,  1927;  Jones,  1957;
Delost and  Delost,  1954;  Quay, 1960; Christian and Davis,   1964; Tahka, 1979).
Having only two immature  animals,  we did  not  include  this  zone in  our analy-
sis.   It  is thus possible that some areas classified as ZR  in females  whose
reproductive condition was not accurately known are in error  in this regard.

     We also assumed that  the sections of adrenal gland examined were from the
center of  each  gland.  Actual  variation in the total cross-sectional areas of
all glands examined supports  this assumption.

     The lipid  content and the presence of  degenerative areas in the adrenal
cortex  have been  frequently  used as  indicators  of adrenal  activity (e.g.,
Andersen and Kennedy,  1932;  Allen,  1960; Dawson  et al. ,  1961;  Christian and
Davis, 1964).   When  the gland is functioning at  "normal"  levels  of activity,
there  is  a large amount  of  cortical  lipid in the form  of  large  droplets; at
higher  levels   of  activity  (e.g.,  under  conditions  of moderate  stess), the
amount  of   lipid  diminishes  and  only  small droplets  may   be  seen.   When the
gland  is overtaxed,  cortical lipid may be  absent,  and degenerative areas are
seen.

     Although  the  tissues were  not prepared by  procedures designed specifi-
cally  to  preserve lipids, we  attempted to roughly  quantify  the  lipid in the
cortex and  the  form  in which  it  occurred.   Observed areas  of degeneration do
not appear to be fixation artifacts.

     Data on male  and female deer mice were treated separately because estro-
gens promote cortical growth in small mammals, whereas androgens retard corti-
cal  development.   Hence,   the  adrenals  of female mice tend to be larger  than
those  of males.   We  also  grouped  females according  to  reproductive   state
(immature,  reproductively inactive, cycling, pregnant,  or lactating) because

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the cortex exhibits periodic fluctuations in size and activity associated with
reproductive condition.  The  cortex  is  large and highly  active  during estrus
and  lactation,  but  smaller and  less active  during  diestrus  and  pregnancy
(Andersen and Kennedy;  1932, 1933).

     Social  and  population  characteristics also influence  the  adrenal struc-
ture of  rodents.  Dominant  individuals have smaller glands than subordinates;
mice in  small populations have  smaller  adrenals than  those in  larger popula-
tions (Christian, 1955; Andrews,  1970).   These  sources of variation are prob-
ably  small  in  deer mice because of  their  relatively  nonaggressive  nature
(Christian and Davis , 1964).
     The mammalian spleen has  many  functions,  including production of red and
white  blood  cells  and  platelets; destruction  of old  or damaged  red cells;
storage of blood; production  of  antibodies;  and the removal of foreign bodies
from the  body  fluids that  circulate  through it.   It can thus be  expected to
detoxify or in  some  cases accumulate  pollutants  from coal combusion that occur
systemically.

     Our measurements in  the  spleen  were designed to estimate its role in the
production and/or storage of blood cells and platelets,  destruction of erthro-
cytes,   immune  responses,  and  the removal of foreign materials  from the body
fluids.  We  suggest that  this  can  be  ascertained by  measuring  changes in
absolute and relative  numbers of  the various  cell  types within  the spleen.
Accordingly,  we identified 40 cells  in the red pulp of each spleen by use of a
reticule with 0.1-mm divisions.  More  specifically,  we  identified the cell at
each  0.1-mm  mark  along  the  reticule in  four  areas  of  red pulp  selected
randomly.

     We also determined:  (1)  The relative  abundance of red  and  white blood
cells  after scanning the entire section at low magnification.  Each spleen was
assigned to one  of  five categories — red cells  far  less,  less, equally, more,
or far  more numerous  than white  cells; (2)  The  amount of hemosiderin present,
determined by scanning  the  section  and then rating  the  concentration of pig-
ment on a  scale  of  0 (none) to 5 (extremely high);  (3)  The number of germinal
centers in the white pulp.  We counted the number present and noted the phago-
cytic  and mitotic activity  within each;  (4)  The number of megakaryocytes and
hemocytoblasts  in section.  In many  cases we counted the number of such cells
in  the section.  Since this  number  depends  somewhat upon the area  of the
section, we also estimated  the abundance of each on a  scale of 0 (none) to 5
(very numerous).

     Our rationale for using the above as measures  of  splenic activity are:

     1.   The relative and absolute  abundance of megakaryocytes are estimators
of the  organ's  role  in  platelet  formation since megakaryocytes produce plate-
lets.

     2.   The relative  abundance  of  red and white blood cells and of erythro-
cytes,  normoblasts,  and  hemocytoblasts in the   red pulp are  estimators of the

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organ's role in the formation and/or storage of erythrocytes.  (Hemocytoblasts
and normoblasts are  immature stages of erythrocytes).

     3.   The  hemosiderin  content of  the spleen is a  measure  of the organ's
role in the destruction of erythrocytes.

     4.   The  relative abundance  of  red and white  blood  cells  and of medium-
and  large-size lymphocytes,  hemocytoblasts, myelocytes and metamyelocytes in
the red pulp  are estimators of the organ's role in white cell production.
(Lymphocytes of these sizes,  hemocytoblasts, myelocytes and metamyelocytes are
immature white cells).

     5.   The  number,  size,  and  mitotic activity  of  germinal  centers  in the
white pulp of the spleen reflect its role in  antibody production.

     6.   The  relative  abundance  of  macrophages,  plasma  cells,  medium- and
large-sized  lymphocytes,  and neutrophils  in the  red  pulp indicate  how much
foreign material is  removed  from the  body  fluids  as  they perfuse the spleen,
since  the  recruitment of  these cells  is  induced  by  such material.   (Macro-
phages  and  neutrophils  phagocytize foreign materials; plasma  cells produce
antibodies;  lymphocytes  produce  antibodies  and   cytotoxic  substances  that
destroy foreign bodies on contact).
Liver

     The vertebrate  liver  has many functions.  For example, it produces bile;
stores  and/or synthesizes  lipids,  glycogen  and  plasma proteins;  and stores
vitamins and  minerals.   It  also detoxifies or removes from the blood numerous
foreign  and  endogenous  substances  including organic  pesticides,  poisons,
hormones and  ammonia.   It  is  thus very likely to  be  directly affected by air
pollutants and to mediate many of the animal's specific responses to pollutant
stress.  Knowledge of the normal structure of this organ in deer mice is prob-
ably essential to the assessment of pollutant-related changes that may develop
at sites of coal-fired power generation.

     We  thus  examined  the liver  to  determine  its  normal structure  and to
identify seasonal  changes, particularly in the incidence of:  (1)  autolysis of
hepatic  tissue  accompanied or not by  cirrhosis;   (2)  glycogen  depletion of
liver  cells  (hepatocytes); (3)  fatty  degeneration  of  hepatocytes; (4)   fat
storage in hepatocytes; (5)  foreign materials and pigment in Kiipffer cells; (_6)
invasion of hepatic parenchyma by foreign bodies and/or inflammatory  cells.

     For purposes of this study, we used the following criteria to distinguish
among  glycogen  depletion,  autolysis  and  fatty   degeneration:   (1)  Glycogen
depletion--Hepatocytes  more  or less  empty and unstained;  only the cytoplasm
surrounding the  nucleus  and   along  the  margins  of  the  cell  is  stained (in
contrast to normal  cells  in  which the cytoplasm  is  uniformly sprinkled with
well-stained  granules); (2)   Autolysis--Hepatocytes  as  above, but  also  with
pycnotic  nuclei;  (3)   Fatty  degeneration--Hepatocytes  with  unstained cyto-
plasmic vacuoles  of variable size (usually small).

     Mild  autolysis  (with little  nuclear change)  could  not be distinguished

                                      233

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from  giycogen  depletion.   Such livers  were arbitrarily placed  in the latter
category.

     The above items,  together  with hepatic blood  flow, were  each rated on a
scale of 0  (none)  to 5 (heavy or pronounced).  The validity of these measure-
ments depends critically on rapid fixation.  Tissue was thus invariably placed
in the fixative within a few minutes  following sacrifice of each specimen.
     The kidney  (in  addition to the liver and  spleen)  is a principal site of
detoxification in the  vertebrate,  and  thus is  likely  to  be directly affected
by inverse pollutants.

     We  examined  the  kidney  primarily  to determine its  normal structure and
associated  pathologies.   Examples  of the  latter are  precipitated protein or
concretions  in the  nephrons,  dilatation  of the  nephrons, changes  in their
epithelial  lining,   degeneration  of  renal parenchyma,  and  the  presence  of
hemosiderin, ascites fluid, inflammatory cells,  or foreign bodies in the renal
tissue.
                            RESULTS AND DISCUSSION

Accessory Sexual Glands of Male Deer Mice

Histology

     The  histology  of the  accessory sexual glands of  several murine rodents
 (e.g.,  house  mice,  voles,  and to  a limited  extent, Peromysous')  has  been
described  (Snell,  1941;  Anthony,  1953;  Lecyk,  1962; Arata,  1964;  Clarke and
Forsyth,  1964;  Hrabe,  1970;  Ewel,  1972).   Our  observations  are generally
similar to  those presented in these earlier studies.  Major differences among
the  glands  occur in the  epithelium  and  in the characteristics  of  the secre-
tion.  All  have  a wall  that consists of a mucosal epithelium that borders the
gland's lumen,  an underlying  connective tissue  (the  lamina  propria), beyond
this a  tunica  muscularis  or coat of smooth muscle, and finally an outer sero-
sal covering.


Vesicular Gland  (Seminal Vesicle).--The  mucosal   epithelium   of  the  active
vesicular  gland  is  a high,  crowded,  simple columnar  layer.  The  cells are
uniformly basophilic with a basal, vesicular nucleus.  They  contain a supra-
nuclear vacuole  of  approximately nuclear size.   This vacuole  contains one to
few  prominent,   large,  deeply  stained  granules  that  resemble  those  in the
gland's lumen.   Many  cells  can  be found discharging these granules into the
lumen.   Such supranuclear vacuoles do not  occur in the other accessory glands.

     The mucosa  is thrown up into primary folds of variable length.  They are
frequently very  long and  narrow, consisting of  little more than two layers of
epithelial  cells  situated back  to back.  Secondary  folds  occasionally occur.
Primary and  secondary folds  sometimes  intersect  forming  a reticulum of epi-
thelial-lined pockets near the margins of the gland's lumen.
                                     234

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     The tunica muscularis  is  thick and heavy  in  the active vesicular gland,
especially in  comparison  with  the muscle layer  of the other accessory sexual
glands.   In  many  places,  it   appears  to  be a  single,  longitudinal  layer.
Elsewhere, it  consists  of an inner circular and outer longitudinal or oblique
layer.

     This  is   the  largest  accessory  sexual  gland.   It  is  comprised  of  com-
pletely  or  partially separated,  adjoining  compartments.   These are separated
from  each  other by inward extensions of the mucosa and underlying muscularis.
The  lumen  is   capacious  and characteristically  filled with intensely eosino-
philic  (bright red)  secretion  in preparations  stained  with haematoxylin and
 eosin.   The secretion   is homogenous  or granular.   So much  is present that it
fills each chamber  and exhibits fractures.

     When inactive,  the  gland  is small with  a  slit-like empty lumen which is
lined  by an inactive,  low columnar  epithelium.   Epithelial cells  are mostly
filled  with  the  nucleus and  exhibit vacuolar  degeneration.   Mucosal  folds
still  penetrate  the  lumen  and compartmentalize the  gland,  and the reticulum
formed by  intersecting  primary and secondary folds may fill the entire lumen.
The  lamina propria  is  densely  cellular  connective  tissue,  relatively  wider
than  that  of  the  active  gland.  Two layers of highly  cellular and dedifferen-
tiated smooth muscle  form  the tunica muscularis.
     Coagulating Gland (Anterior Prostate Gland)--This  compound  tubular gland
nests  in  the  lesser curvature of the  vesicular gland and is somewhat smaller
than  the  latter.  When  active,  its lumen  is  lined  by a simple  cuboidal to
columnar  layer  consisting of  cells with well  defined cell  membranes,  basal
vesicular  nuclei,   and  much  apical cytoplasm  filled  with  fine eosinophilic
granules.  The  epithelial cells  are  brick  red,  in  contrast to those of all
other  accessory  glands.   Each cell  is distinctly  rounded  on  the luminal sur-
face which thus  appears scalloped.

     Small,  widely  spaced   mucosal folds jut into the  lumen  of  the  active
gland.  They  rarely have  secondary  folds.  They tend  to be thick and round, in
distinct  contrast,  for  example,  to the delicate narrow folds in the vesicular
gland.  A thin capsule of circular  smooth muscle (tunica muscularis) surrounds
each  tubule   and  frequently  abuts  on the  epithelium.   The  secretion of the
active  gland  is  granular and only  moderately eosinophilic.   Small, bright red
droplets are dispersed throughout.

     Wh-n  the gland  is  inactive,  its  lumen is tiny,  empty and  lined  by an
epithelium comprised of  (1)  inactive  cuboidal  cells  with large dense nuclei,
and  (2) larger  cells  that  protrude into  the underlying lamina propria.  The
latter  occur  in small groups, commonly adjacent  to mucosal  folds.  They have
considerable  and  poorly  stained  cytoplasm and  central dense  nuclei.  The
lamina  propria  is  thick and highly cellular.  The tunica muscularis  consists
of two layers of highly cellular dedifferentiated smooth muscle.


     Dorsal Prostate Gland.--When  active,   this gland  is a  cluster of  large
acini,  each surrounded by a  thin  capsule of  smooth muscle  (tunica muscularis).

                                      235

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Each  acinus  is  lined by a simple cuboidal or low columnar epithelium.  Nuclei
in  these  cells  are vesicular  and basal.   The  apical  cytoplasm  is  finely
strippled  and eosinophilic.   This gland resembles the  coagulating gland, but
has fewer  folds of the mucosa and smaller tubules.  Some acini have no mucosal
folds.   The  secretion  is  only  faintly  eosinophilic  and  frothy,  but  is
sprinkled with bright red droplets.

      The  inactive gland  is   similar  to  the  inactive  ventral prostrate and
ampullary glands and  will be described with them below.


      Ventral Prostrate Gland.--This compound  tubular  gland  also consists of a
cluster  of tubules,  each surrounded by a thin tunica muscularis.  When active,
each  tubule  is lined  with a crowded simple  cuboidal  to  columnar epithelium,
the cells  of which have basal vesicular nuclei and poorly stained, basophilic
cytoplasmic  granules in haematoxylin and  eosin preparations.  The  height of
the epithelium is inversely related to the volume of secretion in the lumen of
the tubule.  Each tubule is distended with an avidly eosinophilic (bright red)
homogenous  secretion similar  to that  of  the  vesicular  gland.   A  layer of
vesicles frequently  separates  the secretion from the epithelium.  The eosino-
philia,  together  with  the  small cluster of tubules  that  comprise the ventral
prostate gland,  are  diagnostic.  Few mucosal folds occur in  the tubules and
those present are  extemely  small and round.

     Our description of the  ventral  prostate differs  from  that  presented by
Snell  (1941)  for  the house mouse but instead resembles his description of the
ampullary gland.


     Ampullary Gland.--The numerous tubules of this compound gland are notably
large  and  polygonal  in section  when  the gland is active.   The height  of the
epithelium varies  considerably both  among  and within  tubules,  consisting of
low cuboidal  to  crowded  high columnar cells  similar  to those described above
in the dorsal  and anterior prostate glands.  Nuclei  are  vesicular and  basal.
The apical   cytoplasm  is   uniformly eosinophilic.   Many tubules  lack mucosal
folds, but others  have  delicate folds of variable length.  There is almost no
lamina propria, and  the  thin circular layer of smooth muscle that constitutes
the muscularis abuts on the epithelium of each tubule.  Lumens, even in highly
active glands,  are  often empty.   The   secretion,  when present,  consists of
large  masses of a highly  vacuolated homogenous  material,  moderately stained
with  eosin and  confined  to the center of the lumen.  It resembles that illus-
trated by Snell (1941) for the ampullary gland of the house mouse, but differs
considerably from his description of the  gland  (ibid).

     Inactive prostate and ampullary  glands consist of tiny acini with minute
lumens that  are  lined by  a  simple  layer of cuboidal  cells containing dense
nuclei.  Little  and  poorly  stained  cytoplasm is present.   The epithelium is
surrounded by a thick  capsule  of smooth muscle  (tunica  muscularis)  which is
generally highly cellular,  circularly oriented, and dedifferentiated.
                                     236

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Seasonal Changes in the Accessory Sexual Glands of Male Deer Mice

     Quantitative information concerning seasonal changes in the dimensions of
the accessory reproductive glands of deer mice appears in Table 21.1.

     Morton  (in  Lewis et at . ,  1978)  has  shown that  the annual reproductive
period  of  male deer  mice near Colstrip  extends from mid-March through mid-
September.   Testicular  and seminal vesicle weights are  highest between March
and  August,  suggesting  maximal  performance  of  the male  reproductive  system
during  this period.  Kern in the same report  (Lewis et al. , 1978) found active
leydig  cells   in  the testis  between  December  and  the   following  August  and
progressive  increases  in the  diameter of  tubules  in  the  epididymis  between
March and  June,  followed by a brief decline in July  and recovery  in August.
Seminiferous  tubules  in  the  testes  were  also enlarged  between March  and
August.   Development  of  the  epididymis and  seminiferous tubules  depends  on
androgens produced by Leydig cells.  The data suggest that the testes begin to
secrete substantial  and  increasing amounts of androgen in  February or  March,
and  continue to  produce  enough to maintain the reproductive apparatus through
August.

     These findings  concerning the steroidogenetic activity of the testis  are
consistent with  the additional data presented here for  the  seminal  vesicle,
coagulating gland,  and  ventral prostate gland of the same mice.  During 1974,
the  diameter of  the vesicular  gland was high in July  and August,  then dimin-
ished;  diameters of  the  coagulating gland and ventral  prostate were similarly
large between  July  and  September,  then  shrank abruptly.   During 1975,  the
seminal  vesicle was  enlarged  between  April  and  August;  the other  glands
between March  and  August (compare diameters  during 1975  with  those shown  for
October and December of 1974).

     Fluctuations  in the  diameters of  accessory  glands during April, May,
July, and/or August suggest that cyclic discharges of androgen from the  testes
occur during the breeding period.   Changes in the head and tail of the  epidi-
dymis of these mice (Lewis et al-, 1978) support this interpretation,  although
no peaks in size of the epididymis  occur early  in the breeding period.

     Our specimens  tended to  have larger  testes and  seminal vesicles  in  May
and  June  than in  July  and August (Lewis  et al . ,  1978) .  This trend  is  not
present in the histometry of  the  seminal  vesicle,  coagulating  gland,  or ven-
tral  prostate  (Table  21.1).  The  trend is  observed, however,  in the  diameter
of the  seminiferous tubules of immature deer mice; diameter of tubules  in  the
head of the epididymis of immature mice; and in the diameter of tubules  in  the
tail of  the epididymis of adults (see Tables 6.24-6.29, p.  248-253, of Lewis  et
 al . , 1978).

     Our data generally support Morton's suggestion (ibid} that immature males
born  early in the  reproductive  season breed later in  the  same season.  The
size of acini in the ventral prostate gland of immature males in June averages
360.0 [jm  (n  = 2).   This  value is  clearly  within the  size  range of reproduc-
tively  active  adults (March-August  interval  in Table 21.1).   Also,  the dia-
meters  of  the  anterior  prostate  gland and seminal vesicle  of  immature males
are  within or  just below  adult size and sperm  are frequently  present  in  the
seminiferous  tubules and  the epididymis of these males (Lewis et  al. , 1978).

                                     237

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    TABLE 21.1.   SEASONAL CHANGES  IN THE SIZE OF  SELECTED  ACCESSORY SEXUAL GLANDS OF ADULT  MALE Peromyscus
                 maniculatus COLLECTED AT COLSTRIP DURING 1974 AND 1975
00
    Month - Year
                           Diameters of the Vesicular Gland*
Average Diameter
      (Urn)
Maximal Diameter
      (Mm)
   Diameter
of the Anterior
Prostate Gland
     (Mm)
      Values in the table are Means ± SEM (n).
   Diameter
of the Ventral
Prostate Gland
     (Mm)
Jul
Aug
Sep
Oct
Dec
Mar
Apr
May
Jun
Jul
Aug
1974
1974
1974
1974
1974
1975
1975
1975
1975
1975
1975
1968.0
1656.5
1268.6
1398.0
635.8
1380.0
2300.6
1893.4
2034.0
2287.9
2183.3

± 139.1
± 106.1
± 368.6
± 75.1

± 162.1
± 150.2
± 139.7
± 153.1
± 265.7
( 1)
( 5)
( 8)
( 5)
( 4)
( 2)
( 7)
(10)
(18)
(10)
( 7)
2880.0
2265.6
1587-0
1761.6
756.0
2196.0
2904.0
2575.2
2596.0
2800.8
2842.3

± 310.8
± 125.1
± 366.0
± 103.9

± 172.0
± 210.4
± 198.4
± 202.0
± 325.1
( 1)
( 5)
( 8)
( 5)
( 4)
( 2)
( 7)
(10)
(18)
(10)
( 7)
300.0
374.8
300.7
180.6
78.7
366.5
380.9
396.0
314.6
336.6
381.9

±39.1
± 31.3



±47.4
±48.3
±26.8
± 55.5
±85.3
( 2)
( 5)
( 7)
( 3)
( 2)
( 2)
( 7)
( 8)
(12)
( 9)
( 7)
323.8 ± 40.1 ( 4)
252.8 ± 37.8 ( 4)
202.3 + 27.0 ( 8)
119.8 ± 47.1 ( 4)
90.5 ( 2)
272.7 ( 3)
254.3 ± 39.3 ( 7)
356.1 + 31.4 ( 7)
287.3 ± 27.2 (10)
311.4 ± 18.5 (10)
280.1 ± 39.9 ( 7)


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Histology-Preliminary Introduction

     Ova  undergo  limited growth  and two meiotic  cell  divisions  while in the
ovary.  More conspicuous concurrent changes take place within the follicles in
which the ova mature.  In the early developmental  stages, the ova are near the
surface  of  the  ovary and  are  surrounded  by one to few layers  of flattened
"follicle cells"  which,  together with the  immature egg, are called primordial
follicles.  As  the  ovum grows  and  divides,  the surrounding  follicle cells
proliferate  and  become  many  layers  deep  and a connective  tissue   capsule
(theca)  forms on  the outer  surface of the mass.  Thus, a "primary follicle" is
formed.  Liquid-filled spaces now appear among the follicle cells, increase in
size,  and eventually  coalesce  to  form  a  single large cavity  (the   antrum)
within  the follicle.   Follicle  cells now form  a  layer  several  cells in depth
around  the antrum.  This layer is called the zona  granulosa or membrane granu-
losa  and  the  cells are now  called  granulosa  cells.   The theca  is now  thicker
and  consists  of  an inner vascular layer  (theca internal)  containing clusters
of  hormone-producing  gland  cells,   and  an  outer layer  (theca  external)  of
connective tissue and smooth  muscle.   In  contrast  to  the  condition  in most
other  rodents that have  been studied, the  theca  of  the deer mouse is  usually
thin  and  not  well differentiated into layers.  It usually consists of  several
to many layers  of vascular  connective tissue  with few  gland cells and little
muscle.

     We refer to  follicles in which cavities have  appeared and/or coalesced to
form  a small antrum  as  "antral  follicles",  and  those  with  large  antra into
which the oocyte  and an investing layer of  granulosa cells project as "mature"
or  "Graafian  follicles".  There  is  considerable  ambiguity  in  the literature
concerning the names of follicles at various stages of development and  defini-
tions  are thus  particularly important.  Pedersen  and Peters  (1968)  have pro-
posed  a  uniform   system  of nomenclature  to  resolve  the  problem.   Wherever
possible, we have  included their designations for clarity.

     After ovulation,  the  ruptured  follicles  collapse  and  more  or less fill
with  blood from  the ruptured thecal blood vessels and are then termed  corpora
hemorrhagica.  The blood is rather quickly replaced by granulosa cells which
increase  in  size  and  obliterate  the  original  antrum,  transforming  the
follicles  into  an  endocrine gland,  the true  corpora luteum  (TCL)  which pro-
duces progesterone.

     True  corpus  lutea  are  generally nonfunctional, transient structures in
small  rodents such as PeTomysous unless the female becomes pregnant, in which
case  they remain  active  for some time.  Additional follicles in pregnant mice
develop  into  accessory  corpora  lutea  (ACL)  by  a  process  similar  to  that
described for TCL except that  the ova simply  degenerates within the follicle.
We find ACL to be  uncommon in the ovaries  of  deer mice.

     Eventually,  TCL and ACL degenerate.  Cells in the antrum diminish  in size
and  number,  undergo fatty  degeneration, die,  and are  replaced by connective
tissue.  Ultimately, all  that  remains of them  are small nonvascular clumps of
scar  tissue  called  corpora albicantes.   Additional  masses  of  cells  that
secrete  progesterone  occur  in  the  ovarian  stoma.  They may be  of thecal or

                                      239

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granulosa  origin  (Harrison  and  Weir, 1977;  personal observations).   At any
rate, they are  called  interstitial  tissue and are especially prevalent during
late gestation in many rodents.

     Ovarian  follicles  may  degenerate  at  any stage  of development  to  form
atresias  which   are   viable  endocrine  glands   that   produce  progesterone
(Richards, 1978).

     The endocrine component  of  the ovary is thus potentially large, consis-
ting of  estrogen-producing tissue  (thecal gland  cells  and  granulosa  cells),
androgen-producing  tissue (thecal  gland  cells),  and  tissues that  produce
progestins (the granulosa  layer  of  viable follicles;  corpora lutea; artesias;
interstitial tissue)  (Bjersing, 1978; Richards, 1978).
Histology of the Deer Mouse Ovary

     The following histological  characteristics  are diagnostic of the various
stages of follicular development in the deer mouse ovary:

     Primordial follicles  of  deer  mice consist  of  an  ovum  and one  to few
enveloping layers of squamous  (always!) follicle cells, average 24.67 ± 303 |Jm
(x ±  SEM;  n = 18) in diameter,  and characteristically occur in clusters near
the ovary's surface.

     Primary follicles consist  of  the ovum and one to several  layers  of sur-
rounding follicle cells.   If only one layer is present, the follicle cells are
cuboidal or  columnar  (not squamous!).  A theca of  vascular  connective tissue
may be  present.   The egg  itself is frequently surrounded by  a well-defined,
conspicuous  zona  pellucida.  Mitotic  figures  commonly occur  in the  mass  of
follicle cells and  in the theca.  Primary follicles  of deer mice are readily
separated into small,  intermediate, and large categories (Table  21.2).
TABLE 21.2.  DIAMETER OF PRIMARY FOLLICLES OF DEER MICE
                                          Average Diameter        Range of
                                           (|jm ± SEM) (n)       Diameters
Primary follicles of small size 	 39.4 ± 3.6 ( 9)             <50

Primary follicles of intermediate size   . 82.3 ± 3.2 (27)        50 - 105

Primary follicles of large size	150.8 ± 7.9 (18)       106 - 240
The primary  follicles of  deer mice  correspond  structurally to  follicles of
types 3-5 of  Pedersen  and Peters (1968).
                                      240

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     Antral follicles   of   deer  mice  are   generally  larger  than  primary
follicles.  Many  layers of follicle cells surround  the  egg.   Among these are
small  fluid-filled spaces  or  a  small,  frequently slit-like  antrum.   If an
antrum is present,  the cumulus oophorus is broadly attached to the granulosa,
i.e.j it  barely  projects into the  antrum  and most definitely not by a stalk.
A  conspicuous,  but  frequently thin  theca  is also present.   "Early"  antral
follicles contain several small fluid-filled cavities,  whereas "late"  antral
follicles  contain no  antrum.  The  diameters  of  the  two types  differ  (see
Table 21.3).
TABLE 21.3.  DIAMETER OF ANTRAL FOLLICLES
                                          Average Diameter
                                           (|Jm ± SEM) (n)
  Range of
Diameters (|Jm)
Early antral follicles
Late antral follicles
204.2 ± 14.2 (16)
262.8 ± 8.8 (29)
112 - 304
167 - 352

The  antral follicles  of Peromysaus  correspond  structurally to  follicles of
types 6 and 7 of Pedersen and Peters (1968).

     Mature (Graafian) follicles of deer mice are generally so large that they
bulge  from  the  ovary's surface.  The antrum is  large  with a cumulus oophorus
that projects  from a  stalk of granulosa  cells.  The  membrana  granulosa sur-
rounding  the  antrum  is  many  cells  deep.   The  theca  is  broad  and sometimes
divisible  into  internal  and external  layers.   We  have divided  these  mature
follicles into three size classes which presumably represent successive stages
of growth (see Table 21.4).
TABLE 21.4.  FOLLICLE SIZES REPRESENTING SUCCESSIVE STAGES OF GROWTH
                                            Average Diameter
                                             (|jm ± SEM) (n)
   Range of
Diameters (Mm)
Graffian follicles of small size 	  269.3 ±  5.8 (17)      204 - 296

Graafian follicles of intermediate size   .  343.8 ±  5.9 (24)      310 - 391

Graafian follicles of large size 	  534.3 ± 20.0 ( 6)      462 - 592
                                      241

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The mature follicles of deer mice correspond structurally to follicles of type
8 of Pedersen and Peters (1968).

     Corpora hemorrhagica  of  the  deer  mouse  are  generally  ruptured  and
collapsed (or at  least laterally compressed or irregular in shape) and filled
with erythrocytes.  Granulosa cells  more or less crowd  the erythrocytes into
the center of the antrum and obliterate it.

     Corpora lutea of  deer  mice  form when the original  antrum is filled with
large  cells,  presumably of granulosa  origin  (Brambell,  1956).  This "luteal"
tissue  is  highly vascular,  divided  into  small  compartments  by connective
tissue,  and  is  encapsulated by  a  stretched  and  thin theca  in which there is
little distinction between interna and externa.

     We are able to classify the corpora lutea of deer mice into several func-
tional  categories based  on  cytological  characteristics  (see  also  Long  and
Evans,   1922; and  Boling,  1942).   Active  corpora  lutea  (at  peak  secretory
function) contain large round luteal  cells with  well-defined cell membranes;
abundant,  homogenous,  deeply  eosinophilic  cytoplasm;  and  large  vesicular
nuclei with  prominent  nucleoli.   Corpora lutea that have begun  to regress (as
defined  by  Brambell,  1956) contain  vacuelated  luteal  cells.   As regression
progresses,  the number and size of the vacuoles (lipid) increases, as does the
number  of  cells  with  vacuoles.   Nuclei  are unchanged,  but  cell  membranes
become ill-defined.  When completely  regressed and nonfunctional, the corpora
lutea  contain small luteal  cells  that  are  vacant; with  shrunken,  dense  and
pycnotic nuclei;  and  ill-defined cell membranes.   Neutrophils and macrophages
commonly occur  among  the  cells  and there is an increase in connective tissue.
They are also less vascular than active or regressing corpora lutea.

     The corpora  lutea of the deer mouse are  readily classified  into active,
regressive,   and nonfunctional  types  on the  basis of  size,  as  well  as  the
cytological characteristics  presented above (see Table 21.5).
TABLE 21.5.  DIAMETER OF CORPORA LUTEA



                                            Average Diameter      Range of
                                             (|Jm ± SEM) (n)     Diameters (|jm)


Active corpora lutea 	  643.9 ±15.6 (123)    296 - 1221

Regressing corpora lutea 	      (Table 21.6)      314 - 1036

Dysfunctional corpora lutea	337.0 ± 27.4 ( 14)    185 -  574
     We have also been able to distinguish regressing corpora lutea at several
stages  of  involution  on  the  basis  of  their  vacuolation  and size   (see
Table 21.6).
                                     242

-------
TABLE 21.6.
IDENTIFICATION OF REGRESSIVE CORPORA LUTEA BASED ON VACUOLATION
AND SIZE

Degree of Regression
Very mild 	

Mild 	

Mild to moderate . . .

Moderate 	

Moderate to heavy . . .

Vacuole
Size
0
Tiny

Small

Small to
Large
Small or
Large
Variable

Number of
Vacuoles
per Cell
0
1-2

1-f ew

1-f ew

Several
1
Many

Number of
Vacuolated
Cells
0
Few and
Scattered
Many and
Scattered
Most

Most or
All
Most or
All
Average Diameter
(Urn ± SEM) (n)
(Range of
Diameters, (J
0
602.7 + 21.4
(329 to 1036
626.7 + 24.9
(314 to 925)
687.9 ± 28.6
(536 to 832)
659.8 + 22.7
(444 to 925)
578.8 ± 28.5
(500 to 722)

(50)

(40s)

(11)

I"? 71

( 7)


Two  sets  of  corpora lutea were  frequently  found  in a  single ovary.  We define
those belonging to  a single  set  as  those at the same stage of development.  Of
the  89 adult ovaries that we examined, 13.5 percent contained two sets of cor-
pora lutea.  Tn each case, these appeared to be of successive sets.  If one was
fresh and active,  the  other consisted  of  regressing corpora  lutea.   On the
other hand, if one set was regressing, the other was old and dysfunctional.

     Corpora albicantes are  spindle-shaped  collagenous scars of variable size
that frequently occur in large numbers in the ovaries of deer mice.

     Atresias  of  all sizes occur in the  ovary of  the deer mouse.  They exhibit
numerous  signs  of degeneration such as shrunken  oocytes with pycnotic nuclei,
granulosa  cells that  are  sloughing  into the antrum, a collapsed antrum or one
that contains connective tissue cells or inflammatory cells.

     Interstitial tissue  consists  of eosinophilic cells free in the stroma of
the  deer  mouse's  ovary.   The cells  in these irregular well-vascularized masses
have  small dense  nuclei,  abundant  lipoidal or poorly stained cytoplasm, and
indistinct cellular membranes.   They resemble the luteinized cells in dysfunc-
tional corpora lutea.
Seasonal Changes in the Histology of the Ovary in the Deer Mouse

     Seasonal  changes  in the  ovary  of adults  during  1974  and 1975 appear  in
Table 21.7.  Primary  follicles were  numerous  in most ovaries throughout the
year.  Antral and Graafian follicles were also  present in a high percentage  of
cases.  Active  corpora lutea were found in all months except the December-

                                      243

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                                    TABLE 21.7.  SEASONAL CHANGES IN THE OVARY OF ADULT Peromysaus  maniculatus
Month and Year
Item in Ovary
n
Primary Follicles:
% Females Possessing
Females (Number) with
Small 1°F
Intermediate 1°F
Large 1°F
Females Examined
Antral Follicles:
% Females Possessing
Females (Number) with
Early A.F.
Late A.F.
Females Examined
Graafian Follicles:
% Females Possessing
Females (Number) with
fe Small G.F.
*~ Intermediate G.F.
Large G.F.
Females Examined
Corpora Hemorrhagica:
% Females Possessing
Corpora Lutea:
% Females with Active C.L.
% Females with Regressing C.L.
% Females with Dysfunctional C.L.
Females (Number) with C.L. in
Mild Regression
Moderate-Heavy Regression
Atresias :
% Females Possessing
Interstitial Tissue:
% Females Possessing
Jul 74
4

100.0

1
4
3
(4)

75.0

1
2
(2)

75.0

2
3
0
(3)

0.0

50.0
50.0
0.0

2
0

0.0

50.0
Aug 74
7

100.0

2
5
4
(5)

85.7

4
2
(5)

85.7

1
2
3
(6)

0.0

57.1
28.6
0.0

1
1

75.0

14.3
Sep 74
15

100.0

8
15
11
(15)

86.7

9
8
(11)

80.0

2
2
1
(3)

6.7

20.0
60.0
20.0

5
4

20.0

60.0
Oct 74
10

100.0

6
8
9
(10)

60.0

6
3
(6)

50.0

0
1
2
(3)

0.0

50.0
20.0
10.0

1
1

20,0

10.0
Nov 74
8

87.5

5
5
4
(7)

62.5

3
1
(3)

37.5

2
0
0
(2)

0.0

62.5
0.0
12.5

0
0

14.3

50.0
Dec 74
2

100.0

2
1
1
(2)

50.0

1
0
(1)

0.0

	
—
—
	

0.0

0.0
50.0
0.0

1
0

0.0

0.0
Jan 75
3

100.0

1
3
2
(3)

100.0

1
3
(3)

66.7

0
0
2
(2)

0.0

0.0
0.0
0.0

0
0

0.0

0.0
Mar 75
2

100.0

1
2
1
(2)

50.0

1
1
(1)

100.0

1
1
1
(2)

0.0

0.0
100.0
0.0

1
1

0.0

0.0
Apr 75
7

100.0

1
7
6
(7)

71.4

2
5
(5)

85.7

1
0
4
(5)

14.3

42.9
57.1
0.0

3
1

28.6

28.6
May 75
6

100.0

2
6
5
(6)

100.0

1
5
(5)

66.7

0
0
1
(1)

16.7

66.7
50.0
33.3

3
0

66.7

16.7
Jun 75
8

87.5

2
7
5
(7)

50.0

2
4
(4)

87.5

3
1
7
(7)

0.0

62.5
50.0
0.0

2
3

12.5

0.0
Jul 75
8

87.5

5
7
3
(7)

62.5

0
4
(4)

75.0

1
2
5
(6)

0.0

50.0
50.0
12.5

2
2

0.0

37.5
Aug 75
9

100.0

4
7
5
(9)

66.7

2
5
(6)

88.9

0
2
6
(8)

11.1

55.5
44.4
0.0

3
1

11.1

0.0
Supplemental Information:
  % Females Examined That Vfere
    Pregnant or Postpartum

  % Females Examined That Had
    Uterine Scars
75.0
 0.0
         71.4
          0.0
                 28.6
                  0.0
                          57.1
                                   0.0
                          10.0    12.5
                                            0.0
                                            0.0
                                                    0.0    100.0    55.6
                                                    0.0
                                                             0.0    57.1
                                                                             66.7    77.7
                                                                              0.0    37.5
                                                                                              40.0    40.0
                                                                                              25.0    22.2

-------
March  interval  (NB--we lack data for  February).   The  distribution of corpora
lutea  suggests  that  the breeding season extended  from March through December
in  1974,  but was  suspended during winter.  Late  autumn breeding is probably
unusual for  populations of deer mice  in southeastern Montana since it was not
repeated in 1975,  and in 1974 was accompanied by an unusually wet fall (Lewis
e~t at., 1978).  However,  deer mice breed  year-round  elsewhere  (Brown,  1945;
Asdell, 1964).

     The  ovary  during  January  (including  the absence of corpora  lutea),  is
similar  to  that  of voles during  their  nonbreeding  (winter)  season (Lecyk,
1962;  Clarke and Forsyth,  1964; Clarke and Kennedy, 1967; Coutts and Rowlands,
1969), even  though voles seem to be  induced ovulators, and deer mice ovulate
spontaneously (Asdell,  1964).

     According  to Brown  and  Conaway   (1964),  the  corpora  lutea  of Peromysaus
persist for about 2 months postpartum with little or no discernable change in
structure.  Morton (in Lewis et at., 1978)  found pregnant females among deer
mice captured as late as October during 1974.  If corpora lutea persist for at
least  2 months before showing marked regression,  then one would expect to find
them in females as late as December 1974,  which is the case  (Table 21.7).  The
finding of two sets of  corpora lutea in a substantial number of females in our
samples also suggests that corpora lutea persist for some time.  Even in unmated
house  mice,  they  may persist  for two to four successive  estrous cycles (Snell,
1941).

     The  amount  of  interstitial  tissue in  the  murine ovary increases during
late  gestation  (Brambell,  1956).   Thus,  interstitial tissue is  abundant  in
reproductively active  mice.  It was also common in our specimens between April
and   September,    but   conspicuously   absent   through  December   and  March
(Table 21.7).  Atresias were also absent in  the latter months, yet abundant at
times  (June  and  August  1974)  when  interstitial  tissue  was not.   In  other
words, the ovary  of the deer mouse apparently  contained progesterone-secreting
structures only throughout the breeding season.

     It would  seem,  then, that the atretic  follicles  and interstitial tissue
of  deer  mice supplement the corpora lutea  in  the production of progesterone,
which  may be important in  sustaining  pregnancy  after  the corpora lutea begin
to  regress.   We  are  surprised,  however, that  the  incidence  of atresia in any
one  deer  mouse  ovary is as low as it  is (usually confined to one or at most a
few follicles) given the fact that 75-77 percent of all ovarian follicles become
atretic in the ovaries of  rats and house mice  (Arai, 1920; JMandl and Shelton,
1959;  Jones and Krohn, 1961).

     Additional results of the histological survey are the following:

1.   Accessory  corpora lutea rarely  occur  in the ovaries  of  deer mice.  We
found only one clear-cut example in the 89 adult ovaries that we examined.

2.   The  number  of ovaries of immature deer mice available  for study  (11) was
too  small to permit us to  generalize  (Table 21.8).  Notable, however, was the
absence of atretic follicles  and interstitial  tissue in  all  11.  All contained
primary  follicles,  frequently  of  large  size and 10  also  contained antral
follicles.  Six had Graafian follicles, some of which were of advanced age.

                                     245

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  TABLE 21.8.   RELATIONSHIP BETWEEN OVARIAN HISTOLOGY,  OVARIAN WEIGHT,  AND  THE  REPRODUCTIVE STATE OF ADULT AND IMMATURE Peromyscus maniaulatus*^


Reproductive
State
Immature
Adult:
Proestrus
Estrus
Sfetestrus
Diestrus
Anestrus
Pregnant
Immediately
Postpartum
Lactating
Anestrus



N
11

0
4
4
5
15
26
4
11






1°F
90.


100.
100.
100.
100.
96.
100.
90.
.9


,0
,0
.0
.0
.2
,0
9



A.F.
90.9


75.0
75.0
60.0
53.3
65.4
75.0
81.8



G.F.
54.5


100.0
100.0
60.0
26.7
84.6
100.0
81.8



At CH
0.0 0.0


50.0 0.0
0.0 0.0
40.0 0.0
6.7 0.0
26.9 3.8
25.0 0.0
9.1 0.0






Active
0.


50.
50.
40
20
46.
75
27
.0


.0
.0
.0
.0
.2
.0
.3


Very
Mild
0.0


25.0
0.0
40.0
0.0
15.4
25.0
0.0
Corpora Lutea
Regressing
Mild- Mod-
Mild Mod Mod Heavy
0.0 0.0 0.0 0.0


0.0 25.0 0.0 0.0
0.0 0.0 0.0 0.0
0.0 0.0 0.0 0.0
13.3 0.0 0.0 0.0
26.9 3.8 15.4 3.8
0.0 0.0 0.0 0.0
18.2 18.2 36.4 0.0


Int.
Heavy Dys Tiss.
0.0 0.0 0.0


0.0 25.0 0.0
0.0 0.0 25.0
0.0 0.0 40.0
0.0 0.0 20.0
0.0 7.7 19.2
0.0 0.0 25 . 0
9.1 36.4 54.5

Ovary Weight
of Body Weight
Gng/g)*
0.372 ± 0.048


0.425 ± 0.131
0.277 (3)
0.337 ± 0.121 (4)
0.287 + 0.034
0.313 ± 0.028
0.257 + 0.117
0.228 ± 0.051
   * All values except those for ovary weight are the percent of the females in each group that exhibit each item.

   t Abbreviations in the table:  AF = antral follicles;  At = atresias; CH = corpora hemorrhagica;  Dys = dysfunctional corpora lutea; GF = mature
(Graafian) follicles;  Int.  Tiss. = interstitial tissue;  Mod = moderate; 1°F = primary follicles.

   ^ Ovary weights are presented as x ± SEM.   Numbers in parentheses indicate sample size when it differs from that given on the left side of the
table.

-------
Changes in the Histology of the Ovary of Deer Mice During the Estrous Cycle

     Data  (1974-1975) in  Table 21.8  are grouped  according  to  reproductive
state  at time  of capture  (we  will amplify  later on  the  method  we  used to
determine the mouse's  reproductive state).

     Primary  follicles  were  well  represented  at  all  stages  of  the  estrous
cycle, and also  in the  ovaries of immature, pregnant, postpartum,  and lactat-
ing mice.  Atretic follicles were also  common in the ovaries of  reproductively
active females.   Curiously,  active  corpora lutea occur in many  females  at all
stages of  the estrous cycle.  This suggests that corpora lutea  do  not immedi-
ately involute even when the female fails to become pregnant and is consistent
with  Snell's (1941)  finding that the  corpora lutea of house mice  persist for
two to four successive cycles.

     We  were  quite surprised  to  find active corpora lutea  in  the ovaries of
reproductively inactive (anestrus) mice, especially since few of these females
had  Graafian  follicles.   However,  we  expected to  find corpora lutea  at many
different  stages of  regression in pregnant  and lactating  females.   This is
probably related  to the fact that individuals were collected at various  stages
of  gestation (which  lasts  22-27  days)  or lactation (which lasts up  to 4
weeks), intervals in which  the corpora lutea normally degenerate.

     The  average number of  medium to  large  corpora lutea  in  the ovaries of
pregnant deer mice  (5.76 ± 0.01, n = 34) is slightly (0.02 < P  <  0.05;  t-test
using square  root transformations) higher than the number of embryos implanted
in  the  uteri of the  same  mice.  (5.09  ±  0.04),  but is  very  similar  to the
overall mean  litter size of deer mice collected at Colstrip during  1975  (5.75)
(Lewis &t al• > 1978).  These findings suggest that fecundity and fertility are
on  the  average  the  same,  but  that fecundity  frequently  exceeds fertility in
individual  mice.   The  latter  is  typical  of the  bank vole,  C.  glareolus  ,
(Coutts and Rowlands,  1969)  and  has also been reported in two subspecies  of Per-
omysous, P. m. gracilis and  P.  m. bairdii (Asdell,  1964),


Uterine Horn  and Vagina

Histology

     The uterus  and vagina of  deer mice are  structurally similar  to those of
other  species  of  murine  rodents  as  described  by Parkes  (1956).   In both
regions,  the  wall  of  the  reproductive  duct  consists  of  three  layers:  endo-
metrium, myometrium and perimetrium.


Changes in the Histology of the Vagina of Deer Mice During the Estrous Cycle

     Diagnostic  changes  in  the structure of  the  reproductive duct, particu-
larly of its  endometrium,  occur during  the 4 or  5  day estrous  cycle of
deer mice.  These changes  are  similar  to those exhibited  by vaginas of rats and
mice  (Asdell, 1964).  Vaginal smears are also similar (described for the house
mouse by Long and Evans, 1922).  This provides an accurate method  of assessing
the reproductive status  of an  individual deer mouse  and  is the rationale for

                                     247

-------
including detailed studies  of  the vagina in the baseline data for Peromyscus.
In addition,  very early  stages  of pregnancy  are easily  missed during gross
inspection of the uterus,  as  are unattached blastocysts in the uterine horns.
Both are  readily  apparent  in  histological section making  it  possible to more
closely  define  a  female's reproductive  state.   This  is  the  rationale  for
including the uterine horn in the baseline  data.

     The diagnostic  characteristics of the vagina at each stage of the estrous
cycle  of  the deer  mouse  are  presented  in  Table 21.9.  These  are  generally
reliable  for determining reproductive state.  To these,  we add descriptions of
the histology of  the vagina in pregnant  and anestrous  females.   The descrip-
tion for  pregnant animals  is  based on only three mice and is therefore tenta-
tive.  In  all cases,  diagnostic changes occur primarily in the endometrium.

     During pregnancy,  the endometrium is  similar structurally  to  that  of a
female in anestrous  (Table 21.9) except that the epithelial cells may be muci-
fied, as  in  house mice.   The  structure of the  vagina of immature deer mice and
of reproductively inactive adults  is  essentially the  same.   The endometrial
epithelium is only one to three cell layers in depth (NB—this is the most re-
liable criterion for assigning individuals to the anestrous category).  The most
superficial layer consists  of  squamous  or cuboidal cells  with poorly stained
cytoplasm, well defined  cell  membranes and large  oval  nuclei.  The  innermost
layer blends  into the highly  cellular lamina  propria.  The  epithelium lacks
mitotic figures and  rarely contains  leukocytes.  The  underlying and lightly
vascularized  lamina  propria  consists  of dense,  highly  cellular  connective
tissue, and also  lacks  inflammatory cells.   The tunica  muscularis has the two
characteristic layers,  but is thin and undifferentiated.  Its undifferentiated
state is the most  reliable characteristic  for distinguishing between diestrous
and anestrous adults.

     During lactation anestrous, the histology  of the vagina is similar to the
above, except that (1)  the endometrial epithelium consists of three to five
cell layers and contains some leukocytes  (neutrophils and lymphocytes), and
(2)  the tunica muscularis is thick and well developed.

     We cannot emphasize  enough  the necessity  of routinely including sections
of the  vagina in all  future  studies of Peromysous  in  Montana (Table 21.10).
Vaginal characteristics  appear  to provide the most  reliable  information  con-
cerning reproductive  state.


Changes in the Histology of the Uterine Horn of Deer Mice  During the Estrous
Cycle

     The  histological  structure of  the uterine horn is not  a reliable indi-
cator of  reproductive condition in deer mice.  The relevant data are presented
in Tables 21.9  and   21.11.  One  stage grades  almost  imperceptibly  into  the
next.  As in the vagina,  most  of the changes in the wall occur in the endome-
trial epithelium.

     Because most of the  slide  material at our  disposal  consisted of uterine
horns and  so few vaginas  were  included (Table  21.11),  we had  to make infer-
ences about  stages of the estrous cycle for many of our animals  from field

                                     248

-------
                              TABLE 21.9.  HISTOLOGICAI CHARACTERISTICS OF THE UTERINE HORN OF Peromysaus manicutatus
Reproductive
   State
              Endometrial Epithelium
                                                  Uterine Glands
                                     Lamina Propria
                                                                                                                     Tunica Muscularis  Lumen
Immature      Simple crowded cuboidal or columnar Cuboidal to low columnar lining
              layer; nucleus fills most of cell
                                                  Tend to be small in diameter and
              Few mitotic figures                 inactive in appearance
              Few Leucocytes in lining (only
              lymphocytes)                        Lumens usually small and contain
                                                  traces of secretion

                                                  No mitotic figures in lining
                                     Dense,  cellular connective    Densely cellular   Tiny
                                     tissue
                                                                   Undifferentiated,
                                     No mitotic figures            except for layer
                                     No leucocytes in stroma       of numerous and
                                                                   large blood
                                     Lightly vascularized          vessels between
                                                                   muscle layers
Adult:
  Proestrus1
  Estrus
  Metestrus
              Pseudostratified layer
              Traces of vacuolar degeneration

              Moderate numbers of mitotic
              figures

              No leucocytes in lining
              High pseudostratified layer
              Cell membranes well defined

              Moderate numbers of mitotic
              figures

              Variable, but small numbers of
              leucocytes in lining
              High columnar to pseudostratified
              cells, frequently of unequal
              height, their rounded borders
              projecting unevenly into lumen

              Pillar cells (= discharged goblet
              cells) prominent and numerous

              Prominent vacuolar degeneration:
              vacant cells to cells with a
              supranuclear vacuole and above
              that a heavily stained eosino-
              philic layer facing the lumen

              Occasional mitotic figures
Lined by truncated columnar cells

Lumens small and empty

Occasional mitotic figures in
lining



Lined by high columnar cells

Lumens of variable size and contain
traces of secretion

Individual glands highly coiled
(tortuous)

Mild-to-moderate numbers of mitotic
figures in lining

Lined by truncated columnar cells,
some showing vacuolar degeneration

Lumens of variable size with only
traces of secretion

No mitotic figures in lining

Neutrophils and pillar cells in
lining
Dense, cellular connective
tissue

Occasional mitotic figures

No leucocytes in stroma

Lightly vascularized

Highly cellular connective


Occasional mitotic figures

Variable infiltration of
stroma with leucocytes (neu-
trophils and lymphocytes)

Highly vascularized

Dense, cellular connective
tissue

No mitotic figures

Variable, but large infil-
tration of neutrophils in
stroma

Highly vascularized by
numerous hyperemic
capillaries
Densely cellular   Tiny

Just beginning to
differentiate
Well-developed

Highly vascular

Hyperemic
Well developed

Highly vascular

Hyperemic

Variable, but
large infiltra-
tion of neutro-
phils in and
between muscle
layers
Small and
slitlike
Variable:
small to
large in
size
                                                                                                                                      (continued)

-------
TABLE 21.9.  (continued)
Reproductive
   State
              Endometrial Epithelium
                                                  Uterine Glands
                                                                         Lamina Propria
                                                                                                                    Tunica Muscularis  Lumen
  Metestrus   Conspicuous and numerous leuco-
              cytes in lining (ueutrophils and
              lymphocytes)

  Diestrus    Variable:
              Low crowded columnar lining with
              cells of equal height in which
              most of the cell is filled with
              the oval nucleus
                                    Lined by cuboidal or columnar cells

                                    Diameter of glands frequantlv small

                                    Commonly lack a lumen or have
                                    minute lumen
              Epithelium of irregular height with
              rounded peaks and wide or narrow
              valleys, made up of many cells in
              which cell membranes are
              indistinct; nuclei are crowded and
              basal in the lining; superficial
              region of epithelium is eosino-
              philic cytoplasm

              No mitotic figures
              Occasional lymphycytes in lining

  Anestrus    Simple crowded cuboidal or low
              columnar layer

              Nuclei fill most of epithelial
              cells; little cytoplasm

              No mitotic figures
              Occasional lymphocytes in lining
                                     Dense,  cellular connective
                                     tissue

                                     Small numbers of leucocytes
                                     infiltrate the stroma

                                     High vascularity; numerous
                                     hyperemic capillaries
                              Generall well
                              developed,  but
                              beginning to
                              differentiate in
                              some cases

                              Little
                              leucocytosis
                                    Lined by inactive low columnar
                                    cells; sometimes almost cuboidal

                                    Diameter characteristically small

                                    Lumens tend to be small and to
                                    contain traces of secretion
                                     Dense, cellular connective
                                     tissue

                                     No infiltration of
                                     leucocytes

                                     Lightly vascularized
                              As in immature
                              mice
Small and
slitlike
Tiny
Pregnant
(areas other
than in the
sites of
implanta-
tion)
High columnar to pseutostratified
layer
Epithelial cells sometimes of
equal height, but sometimes groups
of cells with basal nuclei and
eosiuophilic apical cytoplasm
collectively drawn out into sharp
high peaks that protrude into the
lumen

Vacuolar degeneration common

Occasional mitotic figures

Occasional lymphocytes in lining
Lined by secretorily active
columnar cells

Lumens of variable, but frequently
large size; empty or contain
traces of secretion

No mitotic figures in lining

Vacuolar degeneration in lining
Dense, cellular connective
tissue

Variable leucocytosis
                                                                                                                     As in metestrus
                                                                                                                                      (continued)

-------
TABLE 21.9.  (continued)
Reproductive
   State      Endoraetrial Epithelium
Uterine Glands
                                     Lamina Propria
                                                                   Tunica Muscularis  Lumen
Immediately   High columnar to pseudostratifled
Postpartum    lining
              Vacuolar degeneration common

              No mitotic figures

              Large numbers of leucocytes in
              lining (neutrophils and
              lymphocytes)
Lining of high truncated columnar
cells

Lumens empty

Lining exhibits vacuolar degenera-
tion and contains variable numbers
of neutrophils
                                     Dense,  cellular connective    As in metestrus
                                     tissue

                                     Marked  leucocytosis (neutro-
                                     phils and lymphocytes)

                                     Extravasation,  in some
                                     places  extreme

                                     Very highly vascular with
                                     numerous small  capillaries
                                     and extreme hyperemia
                                                                                      Large and
                                                                                      distended
Lactation     Simple crowded columnar lining
Anestrus      with cells of unequal height
              extending unevenly into the lumen

              Nucleus occupies most of each
              cell; between it and lumen is a
              conspicuous, but small vacuole

              No mitotic figures
              Occasional lymphocytes in lining
Lined by active truncated, high
columnar cells

Lumens of variable size and contain
traces of secretion

No mitotic figures in lining
Dense, very cellular
connective tissue

Variable, but small
infiltration of leucocytes
in the stroma (neutrophils
and lymphocytes)

Highly vascular
                                                                   Well developed

                                                                   Highly vascular

                                                                   Variable leuco-
                                                                   cytosis in and
                                                                   between muscle
                                                                   layers
                                                                                      Small or
                                                                                      moderate
                                                                                      in size
* This description is based on the uterine horns of two immature mice that were entering proestrus for the first time.

-------
TABLE 21.10.   H1STOLOGICAL CHARACTERISTICS OF THE VAGINA OF Peromyscus
              manioulatus AT VARIOUS STAGES OF THE ESTROUS CYCLE
State of the Estrous Cycle    Diagnostic Histological Features of the Vagina


Proestrus 	  Epithelium consists of a cornified stratified
                              squaraous layer under the surface and a super-
                              ficial layer of mucified cuboidal or columnar
                              cells with pycnotic nuclei

                              Epithelium thick:   14-18 cell layers.  Many
                              mitotic figures in the epithelium.  Few to no
                              leucocytes in the  epithelium

Estrus   	  Epithelium is a cornified stratified squamous
                              layer

                              Epithelium thick:   20-25 cell layers.  Few mi-
                              totic figures in the epithelium.  No leucocytes
                              in the epithelium

Metestrus 	  Initially epithelium is a stratified layer with
                              a sloughing cornified surface; the cornified
                              layers disappear during late metestrus

                              Epithelium thin:  9-12 cell layers.  No mitotic
                              figures in the epithelium.  Leucocytes appear
                              and gradually increase in number in the lamina
                              propria under the  epithelium; later, they become
                              numerous in the epithelium

Diestrus  	  Epithelium is stratified, but not cornified

                              Epithelium thin:  5-6 cell layers.  No mitotic
                              figures in the epithelium.  Mild numbers of
                              leucocytes in the epithelium
                                      252

-------
          TABLE 21.11.  RELATIONSHIP BETWEEN THE HISTOLOGY OF THE UTERINE HORN AND REPRODUCTIVE  STATE  OF FEMALE Peromyscus maniaulatus  *t
Endometrial Epithelium f
Reproductive
State N
Immature 26
Type of
Epithelium
Cu-Co (12)
Co (12)
Co-Ps ( 2)
Number of Presence of
Height Mitotic Imflammatory
(|Jm) Figures Cells
10
0
. 02± 0.40±0.20 0.08 ± 0.06
.53
Type of
Inflammatory
Cells
None
L
(24)
( 2)
Appearance
of Basement
Membrane
D
D-F
F
( 2)
( D
(18)
Vacuolar
Degeneration Number
+ ( 5)
± ( D
- (20)
2.17 ±
0.23
Endometrial Glands
Diameter
(k"n)
22.23 +
0.89
Type of
Epithelium
Cu-Co
Co
( 2)
(22)
Mitotic
Figures in
Epithelium
+ ( 2)
- (24)
Adult:
Proestrus 0 ' ' ' ' ' ' ' ' ' ' ' " ' ' ' ' ' ' ' ' '
Estrus 4-5
Metestrus 5
Diestrus 12
Anestrus 35
Pregnant 25
Immediately 4
Postpartum
Lactation 14
Anestrus
Co-?s ( 2)
Ps ( 3)
Co ( 1)
Co-Ps ( 4)
Cu-Co ( 2)
Co ( 6)
Co-Ps ( 3)
Ps ( 1)
Cu-Co (11)
Co (23)
Co-Ps ( 1)
Cu-Co ( 2)
Cu-Ps ( 1)
Co ( 7)
Co-Ps (10)
Ps ( 5)
Pillar
cells(ll)
Co ( 1)
Co-Ps ( 2)
Ps ( 1)
Cu-Co ( 4)
Cu-Ps ( 1)
Co ( 5)
Co-Ps ( 2)
Ps ( 2)
23
2
22
2
18
1
10
0
18
1
29
3
18
1
.66± 3.1010.71 1.20 ± 0.73
.51
.70± 1.2010.58 3.10 ± 0.78
.34
.50± 0.33±0.26 1.38 ± 0.26
.47
.77± 0.00 0.39 ± 0.08
.45
.82+ 1.02±0.28 1.64 ± 0.30
.13
.75+ 0.7510.48 4.00 1 0.71
.91
.111 0.2510.21 1.57 ± 0.16
.26
None
L
PMN
None
L
PMN
None
L
None
L
None
L
PMN
None
L
PMN
None
L
PMN
( 2)
( 2)
( 1)
( 0)
( 4)
( 3)
( 1)
(11)
(18)
(17)
( 6)
(18)
(10)
( 0)
( 4)
( 4)
( 0)
(14)
( 3)
D
D-F
F
D-F
F
D
D-F
F
D
D-F
F
D
D-F
F
D
F
D-F
F
( D
( D
( 2)
( 3)
( 2)
( 2)
( 5)
( 5)
( 6)
( 7)
(22)
( 7)
(10)
( 7)
( D
( 3)
( 5)
( 8)
+ ( 2)
- ( 2)
+ ( 5)
+ ( 5)
± ( 3)
- ( 4)
+ ( 3)
1 ( 7)
- (25)
+ (14)
± ( 7)
- ( 3)
+ ( 3)
- ( D
+ ( 2)
± ( 3)
- ( 8)
4.40 1
0.24
4.00 1
0.55
3.83 ±
0.34
2.93 1
0.20
3.22 ±
0.26
2.75 +
0.75
4.25 1
0.24
42.20 1
4.82
48.48 +
5.17
34.94 1
2.46
21.53 1
0.76
35.32 1
2.20
46.55 1
4.83
38.38 ±
1.58
Co
HiCo
Co
HiCo
Cu-Co
Co
HiCo
Cu-Co
Co
( 2)
( 2)
( D
( 4)
( D
( 4)
( 4)
( 4)
(31)
Co (14)
Co-HiCo(l)
HiCo ( 9)
Co
HiCo
Co
HiCo
( D
( 3)
( 5)
( 8)
+ ( 4)
+ ( 2)
- ( 3)
- (12)
- (35)
+ ( 3)
- (21)
- ( 4)
+ ( D
- (12)
* Abbreviations  in the table:  AcS =  acellular  secretion;  An = anestrus; C =  cells;  Co = columnar; Cu =  cuboida;  D = distinct; Drv  = debris;
D-F = distinct in  some places, but faded elsewhere; Df = differentiated; Di = diestrus;  EC = epithelial  cells;  Es  —  estrus;  F ~ faded;  I = lumens
of  intermediate  size;  L  =   lymphocytes;  L-D =  lumens that  are  large  and  distended;  Met  = metestrus;  Muc  = mucified;  PMN =  neutrophils;
Pro =  proestrus;  Ps  = pseudostratif led;  RBC = red  blood  cells or  erythrocytes;  S-S1 = lumens that  are  small  and slitlike; St = stratified;
T  = lumens  that  are  tiny;  Tr =  just beginning  to  differentiate;  UDf  = undifferentiated  or  dedifferentiated;  (+) =  present  and  obvious;
(1) = rare; (-) =  absent.

t    Values  in parentheses  in  the  table  indicate  the  number of  mice  exhibiting  the  characteristic  (i.e.,  sample  size);  other values  are
Means t SEM.

£    Mitotic  activity  of  the endometrial  epithelium,  presence  of  inflammatory cells  in the  endometrial  epithelium, the  number  of endometrial
glands,  the amount of  secretion in  the endometrial glands,  the  vascularity  of  the  lamina propria,  the  degree of infiltration of  the lamina
propria with  inflammatory cells, and the amount of material or fluid in the lumen of the uterine horn were  each  rated on a  scale  of  0  (non)  to 5
(very marked or very numerous).
                                                                                                                                       (continued)

-------
TABLE 21.11.  (continued)

Endometrial
Glands*
(continued) Lamina Propria of Endometrium*
Amount of Infiltration Type of
Reproductive Secretion of Inflamma- Inflamma-
State Present Vascularity tory Cells Cells
Immature 0.4810.15 1.96 1 0.21 0.12 1 0.08 None
L


Adult:
Proestrus
Estrus 2.0010.77 2.80 ± 0.49 1.60 + 0.68 None
L
PMN
Metestrus 0.4010.24 3.20+0.58 2.40+0.24 None
L
PMN
Diestrus 1.75+0.33 2.67+0.33 1.08 1 0.34 None
L

Anestrus 1.0910.15 2.27+0.18 0.06 1 0.06 None
L




Pregnant 1.48+0.22 3.52+0.10 2.02 1 0.28 None
L
PMN
RBC





Immediately 1.0010.41 3.25+0.25 4.00 1 0.41 None
Postpartum L
PMN




Lactation 1.5010.27 3.21 1 0.21 1.96 1 0.29 None
Anestrus L
PMN

(24)
( 2)




( 2)
( 1)
( 3)
( 0)
( 2)
( 5)
( 6)
( 6)

(34)
( 1)




( 4)
(19)
(15)
( 1)





( 0)
( 3)
( 4)




( 1)
(13)
( 7)

Width
Myometrium*
Width
(|Jm) (|Jm)
91.29
± 5.




278.
+34.

215.
+48,

202
+29,

106
+ 6,




205.
126,







145,
+40





236
+25


.63




.06
.20

.00
.76

.09
.73

.33
.23




.88
.50







.62
.64





.75
.95


62.
1 2.




134.
115.

162.
+15.

141.
110.

73.
+ 3.




225.
114.







285,
+59





205
+17


31
82




.22
.70

.20
,83

.24
.34

.54
.65




.15
.52







.50
.37





.24
.60


Degree of
Differen-
tiation
UDf (25)
Tr ( 1)




Df ( 4)


Df ( 5)


UDf ( 5)
Tr ( 2)
Df ( 5)
UDf (34)
Tr ( 1)




Df (24)








Df ( 4)






UDf ( 1)
Df (12)


Lumen*
Contents
Size (Amount)
T 0.19 1
0.08




S-S1 0.40 1
0.28

S-S1 ( 3) 0.40 +
I ( 1) 0.40
L-D ( 1)
S-S1 (11) 0.08 +
I ( 1) 0.08

T (32) 0.34 +
S-S1 (3) 0.08




2.00 +
0.38(23)







L-D (4) 1.50 1
0.29





S-S1 ( 6) 0.57 ±
I ( 6) 0.14
L-D ( 1)


Nature of
Contents
None (21)
AcS ( 2)
Deb ( 4)
C ( 1)


None ( 3)
AcS ( 2)

None ( 4)
EC ( 1)

None (11)
AcS ( 1)

None (22)
AcS ( 9)
Deb ( 4)
C ( 5)
PMN ( 1)
RBC ( 1)
None ( 5)
AcS (18)
Deb ( 2)
C ( 4)
PMN (10)
RBC ( 7)
L ( 2)
Sperm (1)
Pigment(l)
None ( 0)
AcS ( 3)
C ( 2)
PMN ( 3)
RBC ( 3)
L ( 1)
Sperm ( 1)
None ( 6)
AcS ( 8)
Deb ( 1)
C ( 1)
Uterine
Weight as
a Function
of Body
Weight
(mg/g)
1.366 1
0.398




2.651 +
0.352

4.317 ±
0.286

2.722 1
0.340

1.173 +
0.114




14.425 1
3.548







16.030 1
3.529





4.195 1
0.536(13)


Repro-
ductive
State of
Vagina
Pro
Di
An



Es


Met


Di


Di
An




Pro
Met
Di
An





Pro
Met





Di
An


( 1)
C 1)
(13)



( 1)


( 2)


( 80


( 1)
(17)




( 1)
( 1)
( 2)
( 1)





( 1)
( 1)





( 2)
( 2)



-------
data on:   (1)  body  and  uterine weight;  (2)  the uterus — scarring, distension
with fluid,  implanted  embryos; (3)  the  vagina--perforate  or  inperforate at
capture;  (4)  condition of the  mammary  glands — conspicuous  grossly or lactat-
ing.  Guidelines  used to  establish reproductive  state  in questionable cases
are these:

     1.    Small  rodents  such  as  Pepomyscus  with  short  estrous  cycles  and
spontaneous  ovulation do  not  have  a  luteal  phase  during  a  typical estrous
cycle.   Hence, the presence of  well developed  corpora lutea probably indicates
pregnancy.

     2.    Reproductively  immature   mice do not  ovulate.   Hence,  a  mouse of
unknown age whose ovary contains corpora lutea  is  an adult.

     3.    Deer mice  have  a  postpartum estrus  during  which they ovulate.  If
fertilized,  the  ova  develop  into  blastocysts,  which  may  remain  free in the
lumen of  the uterine horn for  15-20 days while  the  female  is actively lactat-
ing  (Asdell,  1964).   Furthermore,  females  are  in a state  of anestrous while
lactating.   Hence,  a  deer mouse  whose  uterus  contains free  blastocysts is
probably in a state of lactation anestrus.

     4.    Mammary glands  are enlarged  and  conspicuous  only during lactation.
Hence,  those  females  with conspicuous  mammary glands  are  probably in a state
of lactation anestrus.

     5.    The  vagina  of  the  deer  mouse  is perforate only at copulation and
parturition.   Thus,  individuals of unknown reproductive  state with perforate
vaginas are either in  estrus or  immediately postpartum.

     6.    Mice weighing  14 or  more grams  were  classified  as adults, whether
their ovaries  contained  corpora lutea  or not (see  also  Lewis  et al. , 1978).
Those weighing less  than 14 g, but having  corpora lutea or uterine scars were
also classified as adults,  their small body weights  notwithstanding.

     7.    Vaginal histology  is  a reliable  indicator of the reproductive state
of a deer mouse.

     Using the above  criteria,  the deer  mice  in our sample sort out into the
various  reproductive  classes  described in  Table 21.9 and   21.11.  A few addi-
tional notes are  in order:

     1.    Determination of  the  reproductive state of deer  mice cannot be made
on  the   basis  of distinctness  of  the basement membrane  of  the endometrial
epithelium,  nor  vacuolar degeneration  in the  epithelium,  although these  cri-
teria have been used in studies  of other murine  rodents (e.g., Parkes, 1956).

     2.    The  uterine horn of  the anestrous adult and the  immature deer mouse
are  essentially  the  same  and  represent  the  basal,  undifferentiated state of
the tube.

     3.    The  endometrial epithelium,  and the  glands  derived  from it,  are
especially proliferative (mitotically active) during  estrus.
                                      255

-------
     4.   The acellular secretion  in the lumen of  the  gravid and immediately
postpartum  uterus  is  similar to  that  in  the uterine  glands and  is likely
derived from them.

     5.   The state of the vagina in pregnant females varies  considerably.  In
our limited sample of five vaginas, mudification of the vaginal epithelium was
consistently present,  although such is  reportedly  characteristic of pregnant
house mice (Gorbman and Bern, 1962).

     6.   Changes  in height  of the uterine epithelium of small rodents during
the estrous  cycle are usually subtle,  small,  or  inconsistent  (Allen,  1922;
Allen,  1931;  Clauberg,  1931).  However, (see  Table 21-9),  such  changes  are
among  the more  reliable  discriminating characteristics of the uterine horn of
deer  mice.   The epithelium  is  low  (10-11  |Jm)  during anestrus  and  in repro-
ductively immature deer mice;  intermediate  in height  (18-19  |Jm)  during anes-
trus  pregnancy, and  lactation anestrus;  and high (23-30 pm)  during estrus
metestrus and immediately postpartum.

     7.   Uterine weight is  a  function of body weight  and may also be useful
in  determining  the reproductive  state of  female  deer mice.  This  criterion
allows clear separations  of the following groups,  which are listed in order of
increasing  uterine weights:   (immature  and  anestrus adults) <  (estrous  and
diestrous adults)  <  (adults  in  metestrus or lactation anestrus)  <  (pregnant
and immediately  postpartum adults).

     8.   The maternal and  fetal  placenta of the  deer mouse is similar to the
respective  portions  of the  placenta of the  house  mouse  (described by Rugh,
1968).
Adrenal Gland

Histology

     The adrenal  gland of the  deer  mouse is structurally  similar  to that of
mammals generally  (Bloom and Fawcett,  1975) and  murine  rodents specifically
(Snell, 1941;  Jones, 1957).

     It has  a core of medullary  (chromaffin)  tissue surrounded by a ring of
cortical (interrenal)  tissue.   The medulla  consists of  cords  of  large poly-
gonal  cells  with  vesicular  nuclei and  abundant finely  strippled  cytoplasm.
The cords are  one  or  two cells  across and separated from one another by large
irregular venous channels, which  are typically filled with  erythrocytes.   Even
in preparations stained with haematoxylin and eosin, it is possible to distin-
guish  two  types  of cells in  the  medullary cords.  Most  are a  light burgundy
color.   However, other scattered  cells  are a deep  purple color.  The medulla
is separated  from  the  cortex  by a thin  capsule  of connective tissue which is
frequently difficult or impossible to identify in  section.

     The adrenal  cortex  exhibits  typically  mammalian zonation.  Adjacent to
the medulla  is a  zona  reticularis  (ZR)  of  loosley  packed, polygonal cells,
laced  with  small  vascular  channels  (sinusoids).   The  irregular  packing of
cells  in  this zone is diagnostic.   Cells  tend  to be small  relative to those

                                      256

-------
elsewhere  in  the cortex.   They have vesicular  or dense (sometimes pycnotic)
nuclei.  The cytoplasm  contains moderately eosinophilic granules.  Also found
in this zone are  scattered cells filled with a  golden brown pigment (ceroid).

     External to  the  ZR is a wider zona fasciculata  (ZF) which is composed of
narrow palisade-like  columns  of cells, radially  arranged with respect to the
medulla and separated from one another by fine vascular channels (sinusoids).
Each column is  one  to three cells across  (most  commonly only one cell).  The
cells  are  generally large  and  square.  Nuclei are quite irregular in size and
vesicular.  The  cytoplasm  is  abundant  and filled with eosinophilic granules
giving the cells  a diagnostic uniform red appearance.

     The outermost  and  narrowest region of the cortex is the zona glomerulosa
(ZG) .  It  is not always clearly demarcated from  the  ZF.  It consists of small
clusters  of cells  surrounded  by narrow  vascular channels.  The  cells them-
selves are small  and round with vesicular nuclei and little cytoplasm.

     Sexually immature  and  nulliparous  adult female mice are reported to have
additional  cortical zones, the most common  of  which is the  X zone (Howard,
1927;  Jones,  1957).   These disappear  in adult  males  and  in  females  during
pregnancy.  Such  zones  are most  often juxtamedullary.  So  few immature mice
were available  for study  that we  largely ignored the  X  zone.  However,  our
limited data indicate that an X zone persists in  reproductively active cycling
female deer mice  (n = 3) until  they become pregnant.  It is  absent in pregnant
(n = 6),  postpartum  (n = 1),  and  lactating mice  (n  = 1), as is a ZR.  In its
absence,  the  ZF  is separated  from  the medulla by a  broad  hyperemic  layer of
loosely arranged  connective tissue.  Although no  ZR is present, cells near the
inner  face of the  ZF  frequently have  nuclei that are  smaller than  those in
more peripheral  areas  of  the   cortex.  In contrast,  the  ZR of reproductively
active male  deer mice  is  well-developed, but also  frequently separated from
the  medulla by a  hyperemic  region of  loosely  organized connective tissue.  (We
had  no immature male  deer mice  for comparison with adults.)  Structurally,  the
X zone is  similar to the ZR of adults.

     Cortical cells frequently contain lipoidal  vacuoles of variable size and
number.  Vacuoles also occur in medullary cells in  some cases.

     The entire  gland is  encapsulated by several  closely applied, thin layers
of connective tissue.
Seasonal Changes in the Adrenal Gland of Deer Mice

     Seasonal  changes  in the  histology of the adrenal  gland  are compiled in
Table 21.12, from which we draw the following conclusions:

     1.   The  adrenal gland  rarely  exhibits pathological  changes  in these
populations  of deer mice.  In  our  sample of 72 mice,  only  three had  clearly
diseased  adrenal  glands.  One  exhibited  extensive  fatty  degeneration of the
medulla.  Two  others contained  infiltrations  of neutrophils  in the  ZR.  (Small
infiltrations of lymphocytes do  occasionally occur in the ZR and medulla.)
                                      257

-------
TABLE 21.12.
SEASONAL CHANGES IN THE HISTOLOGY OF THE ADRENAL GLAND OF Peromyscus mamculatus.
THE TABLE ARE MEANS ± SEM
                                VALUES IN

Age/Sex
Group
Adult
Males







Reproductive
Status
Reproductively
Active







Month
Year
Jul
Aug
Sep
Oct
Nov
Dec
Jan
Mar
Jun
74
74
74
74
74
74
75
75
75
n
7
7
7
7
3
4
1
3
2
Total X-sec.
of Adrenal
Sec.
2.12
1.99
2.03
1.78
1.73
1.72
2.10
2.79
1.44
Percent of Total
Cross-Sectional Area Occupied

. (mm2)
± 0.
± 0.
± 0.
± 0.

± 0.



19
17
12
12

06



7
9
8
9
10
15
8
6
16

ZG*
.7 ±
.4 ±
.5 ±
.8 ±
.9
.3 ±
.6
.6
.4



ZF-ZR(X)*
0.4
1.1
1.0
1.4

3.4



79.9 ±
77.9 ±
78.1 ±
74.1 ±
72.6
65.6 ±
88.6
80.0
69.4
3.2
3.9
4.8
2.4

3.7





by

M*
12.4
12.7
13.4
16.1
16.5
19.0
2.9
13.4
14.2
+
+
+
+

+



3.6
3.7
4.9
1.7

1.4



Adrenal
Weight as a
Function of Body
Weight
0.540
0.491
0.552
0.411
0.549
0.602
0.643
0.961
1.000
± 0
± 0
± 0
± 0

± 0



(mg/g)
.093
.044
.055
.038

.084





(5)






M   Immature  Reproductively
^   Females   Inactive
                                    1  1.56
                                       10.3
77.6
12.2
0.677
Adult Anestrus
Females (inactive)
Cycling
Pregnant
Lactating
Anestrus
	 2

4
18
6
2.16

2.46 ± 0
2.39 ± 0
2.81 ± 0


.16
.10
.18
8.0

8.8
10.7
9.9


± 1.4
± 1.6
± 1.8
78.7

79.5 ±
75.3 ±
78.5 ±


4.3
2.2
1.9
13.4

11.7 ±
14.0 ±
11.6 ±
0.424 (1)

3.0
1.6
2.1

0.667 ±
0.696 ±
0.713 ±

0.064
0.078
0.075 (5)
 * ZG = zona glomerulosa;  GF = zona fasciculata;  ZR = zona reticularis;  M = medulla.

 t The degree of vacuolation, degeneration,  or infiltration of cortical  tissue was quantified according
   to the following scale:
              Symbol
               0
           Definition
           None
           Traces or rare
           Some,  several, few,  or mild
           Moderate numbers or  amount
           Many,  numerous,  or heavy
           Very many, very numerous,  or very heavy
    Assigned Numerical Value

              0.00
                                                                               1.
                                                                               2.
                                                                               3.
                                                                               4.
                                                                               5.
                00
                00
                00
                00
                00
                  (continued)

-------
   TABLE 21.12.  (continued)
to
t-n

Cortical Vacuolation
Age/Sex
Group
Adult
Males
















Immature
Females
Adult
Females






Number of
Mice with
Cortical
Vacuoles
(%)
28.6

42.9

28.6

28.6

0.0

75.0

100.00

33.3

50.0

100.0

0.0

0.0

61.1

66.7

Degree of Cortical Vacuolation*,!
Large Vacuoles in
Cortical Cells
0.00

0.29 ± 0.29
ZF (2)
0.00

0.00

0.00

0.00

0.00

0.00

0.00

2.00
ZF
0.00

0.00

0.72 ± 0.30
ZG(1) ZF(5)
0.00

Small Vacuoles in
Cortical Cells
1.14 ± 0.74
ZF(2)
1.43 ± 0.92
ZF(2)
0.86 ± 0.59
ZF (2)
0.86 ± 0.59
ZF(1) ZR(1)
0.00

3.00± 1.00
ZF(3)
4.00
ZF
1.33 ± 1.33
ZF(1)
2.00
ZF(1)
4.00
ZF
0.00

0.00

2.11 ± 0.49
ZF(8) ZR(2)
3.17 ± 1.01
ZF(4) ZR(1)
Degree of
Cortical Degeneration*,!
Pycnotic
Nuclei
2.86 ± 0.59
ZF(2) ZR(4)
0.00

2.57 ± 0.92
ZR(4)
1.14 ± 0.74
ZF(1) ZR(1)
2.00
ZR(2)
3.25 ± 1.11
ZR(3)
0.00

1.67
ZF(1)
0.00

0.00

1.00
ZR(1)
1.50 ± 0.96
ZF(1) ZR(1)
0.22 ± 0.22
ZF(1)
0.33 ± 0.33
ZR(1)
Degenerate
Cells
0.57 ± 0.57
ZR(1)
0.00

0.00

0.00

0.00

0.00

0.00

1.67
ZF(1)
0.00

0.00

0.00

1.00 ± 1.00
ZR(1)
0.00

0.00

Degree
of Lymphycyte
Infiltration* , t
0.29 ± 0
ZR(D
0.00

0.00

0.43 ± 0
ZR(1)
0.00

0.00

0.00

0.00

0.00

0.00

0.00

1.00 ± 1
ZR(1)
0.33 ± 0
ZR(2)
0.00

.29





.43















.00

.23




-------
     2.   Cross-sectional areas  of adrenals  of  adult males  suggest  that the
medulla was more active in October-December 1974 than during other months.

     3.   Monthly differences in the cross-sectional area of the ZF-ZR of adult
males  suggest  that cortical  function  is  relatively  uniform except  in early
winter (December),  when it is reduced.

     4.   On the  basis  of  cortical  vacuolation, more than  25  percent  of  adult
males  appear to  have  been under mild to  moderate  stress during December  1974
and  perhaps in  the January-August 1975  interval.   In  view of this  and the
tabulated  data concerning degeneration  of cortical tissue, adult males appear
to be under mild to severe stress for much of the year.

     5.   Pregnancy and  lactation appear  to  have  imposed  moderate stress on
more than half  of the females in these reproductive states.

     6.   There  is no  correlation between  the   cross-sectional area  of the
ZF-ZR and the lipid measurements for the  same regions of the cortex.

     7.    Changes in the weight of the adrenal gland as a function of the body
weight correspond to changes reported for rats of similar reproductive  stages.
As  reported by Andersen  and Kennedy (1933), adrenal weight is  lowest in anes-
trous  females,  low during  pregnancy,  and highest  at  parturition,  estrus and
during lactation.   In rats,  these changes are associated with  similar  changes
in  the size of the adrenal  cortex, but in deer mice  this  correlation is not
apparent  in the percent of the adrenal  section consisting of  cortex.  However,
it  is  reflected  in  the  actual  areas  of the  ZF-ZR in  the  female population
(Table 21.13).
TABLE 21.13.  AREA OF THE ZONA FASCICULATA AND ZONA RETICULARIS (ZF-ZR) IN
              FEMALE DEER MICE
     Anestrous adults         (n = 2)	1.70          mm2

     Cycling adults           (n = 4)	1.96 ± 0.20

     Pregnant adults          (n = 18)	1.81 ± 0.10

     Lactating adults         (n = 6)	2.21 ± 0.18
                                                   (values are means ± SEM)
     8.   Androgens  are  generally  considered  to inhibit  the  release of ACTH
from  the anterior pituitary  gland of mammals,  whereas  estrogens promote  its
release.  Consequently,  the  adrenals  of  male mammals  tend  to  be smaller than
those  of females  of the  same  species.   However,  this  trend  is  not clearly
shown  in our data for deer mice.   If androgens  inhibit adrenal  cortical func-
                                      260

-------
tion and  presumably size,  then one might  expect changes  in  the  size of the
adrenal cortex and either testes size or the development of androgen-dependent
male accessory sexual  glands  to be inversely related.  Comparison of the data
in Lewis e~t al-  (1978) for the testes and seminal vesicles of our animals with
the data on  the  adrenal cortex  (specifically the  ZF-ZR,  'i.e..,  ACTH-dependent
regions) tabulated  in  this  report illustrates that for months in which sample
size is three to seven, the area of the ZF-ZR and the weight of testes or sem-
inal vesicles are directly related.  All three are elevated in March-September,
then decline to annual lows during December.
Histology

     In general, the  tissue  structure of the  deer  mouse spleen conforms with
that  of mammals  (Bloom and  Fawcett,  1975)  and murine  rodents  specifically
(Snell, 1941;  Elaine and Conaway, 1969).

     The  organ is  encapsulated by  several  layers  of  connective  tissue  and
smooth  muscle,  from which muscular  trabeculae extend  into  the splenic pulp.
In  section,   the  spleen is  long  and  flat  and  trabeculae  tend  to be  most
numerous in the  thinner  regions where they extend  from one  side of the gland
to  the other.  The  prominence of smooth muscle in  the trabeculae, and  the
extension of  the latter  from one side of the gland to the other,  suggest that
they may function to expel  blood from the splenic pulp, e.g . , suggest that the
spleen of Peromysausis a blood cell reservoir.

     The  splenic  tissue  consists  of  red  and  white  pulp.   The white  pulp
(diffuse lymphoid  tissue and  germinal centers) is not usually present immedi-
ately  beneath the  capsule,  but  is  well represented  in the  organ's  center.
Here,  there   are many arteries,  each surrounded by  white  pulp,  arranged  in
tandem  along  the long axis  of  the spleen.  This queue extends from one  end of
the  spleen to the  other.   Additional finer arteries and arterioles surrounded
by thin cuffs of white pulp are numerous and widely scattered throughout the
gland.

     It  is  sometimes  difficult to  distinguish  diffuse lymphoid  tissue  from
germinal centers in the white pulp because all of the lymphoid tissue around a
major  blood vessel resembles  one  gigantic germinal  center.   Accordingly,  we
adopted  the   following  criteria to  distinguish  germinal  centers:   (1)  they
exhibit light  and  dark hemispheres;  and (2) are encapsulated by a dense layer
of reticular  cells and small lymphocytes.  Except for their occasionally large
size,  the germinal   centers  are  histologically  similar  to  those of  other
mammals (see  Bloom  and Fawcett, 1975: 446-561).  They are occasionally packed
with  large  clear  spaces containing macrophages  (with phagocytized  hemosi-
derin), cellular debris, eosinophils, and neutrophils.

     The red  pulp  consists  of   (1) vascular (splenic)  sinuses  lined by simple
squamous  or   cuboidal  cells,  and  (2)  intervening  splenic  cords,  islands  of
tissue  containing  many small  lymphocytes,  reticular  cells,  and macrophages.
Hemosiderin,  when present, is  usually in macrophages within the cords,  rather
than in the vascular  sinuses.   The cords may also house nests of plasma cells

                                      261

-------
and medium to large sized lymphocytes, and occasionally neutrophils.  They al-
ways contain  hemocytoblasts  and megakaryocytes  (occasionally  even metamyelo-
cytes  and  megakaryoblasts),  e.g.,  stem  cells that  produce blood  cells and
platelets,   respectively.   These  stem cells  commonly  contain  hemosiderin.
Since we did  not  see  platelets  (perhaps because  of  the  extreme cellular den-
sity of  the  spleen),  it  is  possible  that  some of  the cells  identified as
megakaryocytes,  especially those with large amounts  of hemosiderin, are multi-
nucleated giant  cells.   However, Snell  (1941) notes  that  megakaryocytes are
conspicuous and  characteristic  of the spleen of  house mice.


Seasonal Changes in the Histology of the Spleen  of Deer Mice

     The data tabulated in Tables 21.14 and  21.15 provide quantitative infor-
mation about  the  red  and white pulp,  respectively,  of the deer mouse at vari-
ous  times  of year.  From  the  tables,  we  make the following general observa-
tions :

     1.   Platelet  formation   occurred  year-round,   but  was  depressed  in
December.   (Observe  changes  in  the  population of megakaryocytes in  the red
pulp.)

     2.   Erythropoiesis  and/or storage  of erythrocytes  in  the spleen was
elevated in July-August  1974.   (Note  rations  of red  to  white  blood  cells and
the  percent  of  the spleen cells in the red pulp represented  by erythrocytes
and normoblasts.)

     3.   The destruction  of  erythrocytes was elevated in  May  and  June, and
the  August-October interval.    (This  conclusion  is  based on  the hemosiderin
content of  the spleen.)

     4.   Lymphopoiesis  was  elevated   during  September-November.   (Note the
percent  of  the  cellular population  represented by  medium  and  large  sized
lymphocytes.)

     5.   The number of foreign bodies trapped in the  spleen and the antibody
production  of the  organ was  high  in August-November  and perhaps  in June.
(This  is suggested by  the numbers  of macrophages,  neutrophils, plasma cells,
and  medium  to large  lymphocytes in the red pulp,  as well  as  the number and
mitotic activity of the germinal centers in  the  white pulp.)

     6.   On  a  seasonal  basis,  splenic weight  declines during  November and
December.  Spleen weight also shows considerable individual variation  in Per-
 omysous ,  ranging between 1.498 and 16.337 mg/g of  body weight.  Such  large
variation is  not  unexpected  (see Skryja and Clark, 1970).  In house mice, for
example, splenomegaly  is  found in subordinate males,  in distinct contrast to
dominant individuals,  and is  accompanied systemically  by  anemia  and histo-
logically by  marked  reduction  in  the white pulp, and increased formation of
erythrocytes  and megakaryocytes in the red pulp  (Elaine and  Conaway,  1969).
However, if  the differences  in  spleen weight  in deer mice  are  a function of
social status, then we might expect to find the following in enlarged spleens:
(1) low percentages of small lymphocytes;   (2) high percentages of erthrocytes,
megakaryocytes,   hemocytoblasts,  and  normoblasts  in  the red pulp;  (3)  large

                                     262

-------
TABLE 21-14-  SEASONAL CHANGES  IN THE HISTOLOGY OF RED  PULP  IN THE SPLEEN OF  Peromysaus  manioulatus.   AGE AND SEX  CLASSES ARE COMBINED  IN EACH
              MONTH.  CELL  POPULATIONS  ARE EXPRESSED AS A PERCENT OF THE TOTAL CELLS PRESENT UNLESS OTHERWISE INDICATED.  VALUES ARE MEANS ± SEM









Month-
Year
Jul 1974

Aug 1974

Sep 1974

Oct 1974

Nov 1974

Dec 1974

Jan 1975
Mar 1975

May 1975
Jun 1975

Jul 1975
Aug 1975


fa
CO T3 CO i— 1
QJ -O Q) QJ rH
4-> O N 4-1 V
>» CO -H >. CJ
U CQ U
O S 1 O CO
H A 3 OJ A B
rH O, 'H W 0. a
CO |3 -O H [3 CO
n ti S a i3 tn- ft!
12 26.7 4.6 0.0
±3.6 ±2.4
19 26.4 6.0 0.1
±3.5 ±1.0 ±0.1
19 22.2 13.9 0.1
±1.9 ±2.3 ±0.1
13 20.7 9.4 1.1
±3.3 ±2.0 ±0.4
6 19.6 14.2 0.4
±2.3 ±2.6 ±0.4
4 18.8 3.1 0.0
±5.8 ±1.6
1 22.5 5.0 0.0
6 35.0 4.6 0.0
±5.7 ±1.5
3 26.9 3.3 0.0
7 26.9 2.5 0.0
±4.3 ±1.1
1 35.0 7.5 0.0
4 19.0 4.1 1.2
6.2 ±1.1 ±1.2
* Subjective ratings concerning the
hemocytoblasts , and the amount of
been




+
++


w
QJ
t>0
(3
J3
ft
O
IH
u
a
4.2
±1.4
5.1
±0.9
7.8
±1.6
9.7
±1.6
10.0
±1.9
8.8
±4.3
7.5
9.6
±1.9
17.8
21.1
±2.7
7.5
17.6
±4.4
number of
T3
d
«

CO cfl
l-H rH
•H -H
JS Jl
& o.
0 0
u a
4-1 -rt
S co
QJ O
z w
0.4
±0.3
0.5
±0.3
2.4
±0.6
3.0
±1.0
2.5
±1.3
1.2
±0.7
0.0
0.4
±0.4
0.0
1.8
±0.9
0.0
0.0


io
QJ in
4-1 4-1
r-> CO
0 CO
O r-t
H f
ja o
h g
t? 0
W K
40.1 0.2
±2.9 ±0.2
35.0 0.0
±2.4
21.1 0.1
±2.4 ±0.1
20.3 0.0
±2.7
20.8 0.0
±3.5
26.2 0.0
±2.2
17.5 0.0
19.6 0.0
±2.6
28.4 0.0
21 . 4 0.0
±3.4
12.5 2.5
24.4 0.0
±6.9
megakaryocytes and
en
4J
CO
>
u
§
OJ
1.2
±0.6
0.5
±0.2
0.6
±0.2
0.8
±0.4
1.7
±0.8
0.9
±0.6
0.0
1.7
±0.5
0.0
1.4
±0.7
2.5
2.4
±1.0
**
hemosiderin, in each spleen have
transformed into numerical equivalents
Rating Scale
0 = none
± = traces (rare)
+ = mild (some or few)
+ = moderate
+ = heavy (many or numerous)
of this
summary, viz:

CO
H QJ
O 4-*

W U
OJ O
4-1 rH
>> OJ
U >>
o e
rH CO
QJ 4-1
£>> OJ
as
0.0

0.0

0.1
±0.1
0.0

0.0

0.0

0.0
0.0

0.0
0.0

0.0
0.0

Subjective
Cfl
i-H
W rH
U rH QJ
QJ rH CJ>
4-1 OJ
>-. U rH
U CO
O ^4 -H
>> CO rH
£4 rH QJ
Ctj 3 J3
jj U 4-1
CO -H O
00 4-1 TJ
QJ QJ d
0.8 14.9 6.0
±0.4 ±1.6 ±1.4
0.4 16.6 7.5
±0.2 ±2.1 ±1.1
0.4 20.4 9.2
±0.2 ±1.9 ±1.2
0.2 22.7 11.0
±0.2 ±2.3 ±1.6
0.4 17.5 12.5
±0.4 ±1.9 ±2.5
0.0 30.0 10.0
±7.9 ±1.0
0.0 37.5 10.0
0.0 21.7 6.2
±3.5 ±1.9
0.8 15.5 5.7
0.0 19.3 5.0
±2.1 ±2.2
0.0 17.5 15.0
1.1 21.4 4.0
±1.1 ±6.6 ±1.0
ratings of the ratio
*
CO
QJ QJ
rH 4-1
U !>>
CO U
3 0
a >>
u
,d co
4-1 M
O to
O CJC
S a1
0.4 1.83
±0.3 ±0 . 34
1.8 1.63
±0.4 ±0 . 22
1.6 1.68
±0.4 ±0.31
1.1 1.23
±0.5 ±0.23
0.4 1.67
±0.4 ±0.33
1.2 0.50
±1.2 ±0.29
0.0 1.00
1.2 2.33
±0.6 ±0.80
1.6 1.33
0.7 1.86
±0.5 ±0.70
0.0 1.00
4.7 3.50
±1.0 ±0.50
•i!
(0
4-1
CO
CO
r— I
,0
O
4-1
>l
U
O
B

2.67
±0.43
2.42
±0.26
2.37
±0.32
2.23
±0.38
2.83
±0.48
1.00
±0.41
4.00
4.17
±0.40
3.67
2.67
±0.71(6)
4.00
3.50
±0.50


d
>H
ti
QJ -K
TJ 4-1
•H d
CO QJ
0 4J
B d
QJ O
1.75
±0.33
2.26
±0.27
3.00
±0.30
2.27
±0.34
1.67
±0.44
1.25
±0.63
0.00
1.25
±0.25
3.83
3.36
±0.28
0.00
3.25
±0.32
of erythrocytes to leucotytes in
red pulp of the spleen have been transformed
alents for
Numerical Equivalent










++-H- = very heavy (very numerous)
0
1
2
3
4
5












£
0 S
4J ^
«
CO * — '
QJ
4-> CO
>. QJ
m u 4-1
o o >>
l-< U
0 XI 0
•H 4-1 U
4-1 >> a
(5 U OJ
ffn W 1— 1
1.33
±0.17
1.13
±0.12
1.03
±0.13
1.35
±0.16
1.25
±0.21
1.38
±0.24
0.50
1.00
±0.18
1.33
0.93
±0.07
0.50
1.12
±0.43
the
into numerical equiv-
purposes of this summary, viz:
Rating Scale
R « W
R > W
R = W
R > W
R » W

Numerical
0
0
1
1
2

Equivalent
.0
.5
.0
.5
.0
















-------
TABLE  2L15.  SEASONAL  CHANGES  IN THE  HISTOLOGY OF  WHITE PULP IN THE  SPLEEN OF Peromyscus manieulatus.
              AGE AND SEX CLASSES ARE COMBINED IN EACH MONTH

Germinal Centers in White Pulp
Month-
Year
Jul
Aug
Sep
ro Oct
ON
Nov
Dec
Jan
Mar
May
Jun
Jul
Aug
1974
1974
1974
1974
1974
1974
1975
1975
1975
1975
1975
1975
n
12
20
19
13
6
4
1
6
3
7
1
4
Total
f x "*~
16
13
18
16
25
13
14
17
12
15
14
20
.67
.00
.21
.31
.83
.75
.00
.67
.33
.57
.00
.75
Number
SEM)
± 1.91
± 1.18
±2.75
±2.02
± 4.75
+ 2.56

± 2.70

±2.26

±2.46
Number with Pronounced Spleen Weight as a
Mitotic Activity Function of Body Weight
Range and/or Lymphoblasts in mg/g (x ± SEM)
3 -
3 -
4 -
4 -
14 -
8 -

12 -
4 -
7 -

17 -
27
23
51
31
44
19

26
17
24

28
0
0
0
0
2
0
0
1
0
0
0
2
4
4
4
3
3
2

4
4
6
4
5
.545 ± 0.469
.192 ± 0.475
.966 ± 1.240
.899 ± 0.993
.376 ± 0.451
.128 ± 0.271

.521 ± 0.907
.224
.860 ± 1.433
.323
.411 ± 0.471

(14)
(11)






( 6)



-------
numbers of megakaryocytes  and hemocytoblasts in the red pulp;  (4) high red to
white blood  cell  ratios;  and (5) relatively few germinal centers in the white
pulp.  In only  four  of the 12 mice with splenomegaly did three or more of the
above characteristics  occur.  It  appears that social status  and  other as yet
unidentified  factors  contribute  to  differences  in the  size  and  histology of
this organ in deer mice.   For example, four of the five females with enlarged
spleens were  pregnant.
Liver

Histology

     The  deer  mouse liver  is structurally similar  to  that  of mammals  (Bloom
and Fawcett, 1975)  and mice  specifically  (Snell,  1941).  It consists of large
"classical" lobules that are  indistinctly separated from one  another by connec-
tive tissue.  Where three lobules meet, they form a space, the triad, contain-
ing  branches  of  the  hepatic artery,  portal  vein,  bile ducts  and lymphatic
channels.  Radially arranged  vascular  channels (sinusoids)  carry blood toward
the  center  of  each lobule  and anastomose there to  form  a  central  or hepatic
vein.   Sinusoids  tend  to   be narrow and  are  sometimes  difficult  to  locate.
They are lined by a simple  squamous endothelium and large, conspicuous Kiipffer
cells  which project  into   the lumen.  They  are  commonly   filled  with  blood
cells,  which were frequently  refractile, poorly  stained  and had considerable
associated hemosiderin.  This  suggests that blood stood in the tissue for some
time before fixation.   Characteristics  of the liver cells are consistent with
this  interpretation.   Kiipffer cells  also commonly  contained  hemosiderin  and
occasionally black specks which we assume are particles  of  carbon.

     Each lobule is composed  of large, polygonal hepatic  cells that are organ-
ized  into  cords  or plates  that  radiate  like  the fins  of a  paddle  wheel from
the central vein  to the edges of  the  lobule.   Each hepatic plate is one cell
across  and  separated  from  the next by  a  sinusoid.   The liver cells or hepto-
cytes  in the  plates  have   finely  strippled  cytoplasm  and one or two nuclei.
They  are sometimes  vacuolated  (infiltrated  with  fat),  have  poorly stained
cytoplasm  (indicating  hydropic  degeneration  and/or  glycogen  depletion)  or
pycnotic nuclei (indicating cellular degeneration) or contain a  brown pigment.

     Autolysis was frequently present  in our  liver   samples.   However,  the
observed pattern  varied considerably from one liver to another.  These varia-
tions  may  indicate shifts  in blood  flow through the  liver as  a function of
processing at or near the mouse's death.

     The  liver was  also  commonly infiltrated  by small focal  aggregates of
lymphocytes, usually near the  triads.

     Several livers exhibited pathological changes such  as cirrhosis (n = 1) ,
epithelioid replacement of  hepatic tissue  (n = 2), infiltration of the hepatic
parenchyma  by  giant  cells  (n =  1),  cocci with or without  inflammatory  re-
sponses  (n = 3),  and  localized hepatic  degeneration accompanied by inflamma-
tory responses  (n  = 2).
                                     265

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Seasonal Changes in the Histology of the Liver of Deer Mice

     Seasonal  changes  in  the  histology  of  the  liver  are  summarized  in
Table 21.16, from which we  draw the following inferences:  1.  Fat storage in
the  liver  was  uncommon;  2.   In contrast,  lymphocyte  infiltration,  usually
focal in nature and largely restricted to the triads, was common; 3.  Glycogen
depletion,  widespread  when  present, occurred  during July-September  1974;  4.
Widespread  autolysis  was common,  especially  during December  1974  and June
1975; 5.  Pathologies were most common during September 1974.  In combination,
items 3-5 suggest that the energy demands and/or sources of stress on the mice
were  unusually  high  during  June-September  and  December.  Results  of  the
adrenal  survey  (changes  in  cortical  lipid) are  consistent with  this  inter-
pretation:   they suggest  that  the  mice were under  considerable  stress  during
December 1974 and January-August 1975.

     6.   Kiipffer cells contained  the  most hemosiderin during May  and  August
1975  (but not  during  August 1974).   If this reflects erythrocyte destruction,
then the latter  was  high  during the same months,  and erythropoiesis might be
expected to  rise shortly thereafter.  The  results  of  the spleen  survey are
consistent  with this  interpretation:   they  suggest that  erythropoiesis  was
high  in July  and  August  and  that  erythrocyte  destruction was high  during
May-June and August-October.

     7.   Blood flow through the liver  was elevated during September, October,
and  December  1974,  and March  1975,  but reduced  in May-August  1975.  Whether
this reflects real differences  in  liver  function or  simply variation in pro-
cessing of the tissues (e.g., the time  of day when the mice were killed or the
speed with which the liver was fixed) is unknown.
Histology

     The histological structure of  the  kidney of deer mice generally conforms
to descriptions presented in standard references (Bloom and Fawcett, 1975).

     Renal corpuscles  are  mammalian  in  type with a  simple  squamous Bowman's
capsule and  glomerular  capillaries.  The juxtaglomerular apparatus  is  a con-
spicuous feature of the vascular pole of many of them.

     The  proximal  portion  of  the  renal tubule  consists  of convoluted  and
straight regions.  The latter is considered  to be the descending thick limb of
the loop of Henle (Bloom and Fawcett, 1975).

     1.   Convoluted  region—this  is a  round,  relatively large  tube,  lined
with a simple high columnar epithelium that  has a conspicuous brush border and
radial striations in the basal region of the cells.  Their cytoplasm is avidly
eosinophilic.  The nuclei  are sharply defined, but variable in position in the
cell.  The lumen of the tubule is  irregular,  either large and  oval or slit-
like.  Proximal convoluted tubules are especially numerous in the outer cortex
of the deer mouse kidney.
                                     266

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TABLE 21-16.  SEASONAL CHANGES  IN  THE HISTOLOGY OF THE LIVER  OF Peromyscus maniaulatus .*  VALUES IN THE
              TABLE ARE MEANS ± SEM.  SEX AND AGE GROUPS HAVE BEEN COMBINED
 Month-
  Year
    Characteristics of Hepatocytes

   Fatty       Glycogen
Infiltration   Depletion    Autolysis
                                                                                     Pathology
                           Pigment Content
                          of KUpffer Cells
                                 Lymphycyte
                                Infiltration
                                   Hyperemia
Jul 1974   13

Aug 1974   20

Sep 1974   16

Oct 1974   14

Nov 1974    6

Dec 1974    4

Jan 1975    1

Mar 1975    6

May 1975    4

Jun 1975    7

Jul 1975    1

Aug 1975    4

Grand Mean ±
SEM (n = 12)
0.31 ± 0.13

0.25 ± 0.16

0.19 ± 0.19

0.29 ± 0.16

0.00

0.00

0.00

0.33 ± 0.21

0.00

0.00

0.00

0.00
1.62 ± 0.51  0.85 ± 0.52

0.65 ± 0.31  0.60 ± 0.17

1.62 ± 0.52  0.88+0.33
0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00
0.71 ± 0.29

0.83 ± 0.48

3.50 ± 0.87

1.00

1.33 ± 0.56

2.00 ± 0.47

3.17 ± 0.91

1.00

1.25 ± 0.63
0.46 ± 0.14

0.35 ± 0.17

0.00

0.92 ± 0.51 (13)

0.50 ± 0.22

0.25 ± 0.25

0.00

0.17 ± 0.17

3.50 ± 0.78

1.29 ± 0.61

0.00

2.75 ± 1.30
0.85 ± 0.22

0.60 ± 0.17

0.40 ± 0.20

0.79 ± 0.39

0.50 ± 0.22

0.00

0.00

0.17 ± 0.17

0.00

0.57 ± 0.57

0.00

0.25 ± 0.25
1.69 ± 0.60

2.00 ± 0.46 (19)

4.62 ± 0.20

3.57 ± 0.39

2.33 ± 0.95

5.00 ± 0.00

0.00

3.67 ± 0.67

0.75 ± 0.75

0.14 ± 0.14

0.00

0.75 ± 0.75
0.11 ± 0.04   0.32 ± 0.18  1.43 ± 0.28   0.85 ± 0.33
                                             0.34 ± 0.09   2.04 ± 0.52
*  Each histological characteristic  in  the  table has been estimated  on  a scale of 0  to  5,  according to
which  0  =  absent;  1 =  mild;  3 =  moderate;  and 5 = heavy  or pronounded.   The values in  the table are
averages of values assigned to the animals in each monthly sample.

-------
     2.   Straight region--This  region is similar  structurally  to the convo-
luted  region,  but is  somewhat  smaller in  diameter.   The epithelium  is also
lower, consisting of simple cuboidal or low columnar cells which have the same
high  affinity  for eosin,  basal  striations, and  brush border.  The  lumen is
round  or oval.  These  tubules  lie in clusters within  the inner cortex and at
the junction of the cortex with the medulla.

     Loops  of Henle  are  very  narrow,  round  tubules with  a  thin,  simple
squamous lining.They occur in groups of 12 to 15 among thick limbs (proximal
and  distal)  and  collecting tubules.   They can be  recognized by  their small
diameter and  the  fact  that they are accompanied by vasa rectae,  capillaries
filled  with red  blood cells.    (This  portion  of the  renal  tubule  is  tradi-
tionally called the thin limb of the  loop of Henle.)

     The distal portion of the  renal tubule, like its proximal counterpart,
has  a  convoluted  and  a straight region, the  latter being the ascending thick
limb of the  loop of Henle.

     1.   Convoluted region—This region of the tubule  is  round in section and
somewhat smaller than its proximal counterpart.  It occurs in the same general
area,  however.   Groups  of  these  tubules  are  frequently  interspersed  with
groups of proximal  convoluted  tubules in the  cortex.   They  are  recognized by
their  simple   cuboidal  to  low  columnar epithelium,  the  cells  of  which  are
characteristically  irregular  in height  and  have  poor  affinity  for  eosin,
granular cytoplasm, and lack of brush border.  The lumen of this region of the
renal tubule is slit-like and stellate-shaped in section.

     2.   Straight region--Histologically,  this region  of  the tubule resembles
the  distal  convoluted  region,   but  is somewhat  smaller  in diameter.   It  is
lined  by a  simple  squamous or  low cuboidal epithelium,  consisting  of poorly
stained, granulated cells.   In contrast to the convoluted  region of the distal
tubule, the lumen  is  round,  generally empty,  and has  an  epithelial lining of
uniform  height.   Straight  regions  of the  distal  tubule  occur  in  the  outer
medulla and  bordering inner cortex.

     Renal  tubules are connected with a system of collecting tubules including
collecting and papillary ducts.

     1.   Collecting ducts—These  occur in  the  medulla  and extend  into  the
cortex as medullary rays to pick up  the more  peripheral  renal tubules.  They
are  round  in  section  and  relatively  small  with a simple  cuboidal  (in  some
places  almost squamous)   lining.   The  epithelium  is  characterized  by  its
irregular height,  and  its cells  by their lack of staining  (vacant cytoplasm);
they  have well defined cellular membranes  and contain a  large, well defined
nucleus.

     2.  Papillary ducts--These are  large,  round or  oval  tubules  that  are
lined with a simple low cuboidal or columnar epithelium.  Epithelial cells are
similar  to  those  lining  the  collecting ducts,  but  may  also contain  a  few
stained granules.   The lumen is small and polygonal in shape.  Papillary ducts
are confined to the medulla, especially to the papilla.
                                     268

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Seasonal Changes in the Histology of the Kidney of the Deer Mouse

     Seasonal  changes  in  the  histology  of  the  kidney  are  compiled  in
Table 21.17.  The  data suggest  that proteinuria commonly occurs in the kidney
of deer mice; that concretions are rare; and, as expected, that hyperemia is a
constant feature of the kidney.

     We found many cases  (n = 10) in which blood had pooled in the kidney for
some time.  Blood vessels were choked with poorly stained, refractile erythro-
cytes and hemosiderin.  We  suspect that these are fixation artifacts.  Consis-
tent with these  observations  is the fact that many of the kidneys were poorly
fixed.   Pycnosis,  for example, was  commonly widespread,  particularly in the
deeper regions of the  kidney.

     The kidney frequently  (44.4 percent) exhibited pathological changes.   The
incidence of pathology exceeds 50 percent of the sample in September, October,
and November, 1974 and in May, 1975.  The most common pathology (28.4 percent
of our sample) was focal lymphocyte infiltration.   In only five cases did lympho-
cytes surround foreign bodies (bacilli).  However,  they were frequently accom-
panied by other types of inflammatory cells, such as macrophages,  neutrophils,
and in one case plasma cells.   Lymphocytic infiltration was confined to the
renal cortex and the distribution of lymphocytes there suggests that they arose
by perivascular cuffing.

     Epithelioid  replacement  of  renal tubules  occurred  in  three  mice.   In
these animals,  the renal  tubules  were solid cords  of cells encased by lympho-
cytes and neutrophils.  The kidneys of two  other mice  exhibited  intertubular
edema.
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                                      269

-------
  TABLE  21.17.  SEASONAL CHANGES IN SELECTED ASPECTS OF THE KIDNEY OF Peromysaus mani.cula.tus.*  SEX AND AGE CLASSES ARE COMBINED IN EACH MONTH

Month-
Year
Jul 1974

Aug 1974

Sep 1974

Oct 1974

Nov 1974

Dec 1974

Jan 1975
Mar 1975

May 1975

Jun 1975

Jul 1975

Number of
n
13

19

15

11

6

3

1
6

4

2

1

PCT
0

7

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7

2

1

1
2

0

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1

PCT-I
5

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0

0

0

0
0

0

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Mice with Protein In*
DCT
0

1

8

5

3

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3

1

1

1

DCT- 1
1

0

0

0

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LH
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0

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RC
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1

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0

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Number of Mice with
Concretions In*
PCT
2

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0
0

0

0

0

LH
1

0

0

0

0

0

0
0

0

0

0

Degree of
C
2.56 ± 0.31
(9)
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(10)
2.46 ± 0.41
(13)
1.25 ± 0.53
(8)
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(5)
4.00
(2)
2.00
2.00 ± 0.82
(4)
3.00
(3)
4.00
(1)
4.00
(2)
M
2.33
(3)
2.50
(2)
1.25 ±
0.72(4)
0.00
(4)
0.00
(2)



0.00
(1)
3.00
(1)




Hyperemia In*,
(C)(M)
3.00 ± 0.58
(4)
3.78 ± 0.22
(9)
1.33
(3)
0.86 ± 0.40
(7)
0.67
(3)
4.00
(1)

2.00
(3)
4.00
(1)
2.00
(1)
2.00
(2)
,t
Whole Kidney
2.68 ± 0.28

3.45 ± 0.20

2.53 ± 0.37

1.45 ± 0.39

2.00 ± 0.73

4.00

2.00
2.33 ± 0.61

3.25 ± 0.48

3.00

3.00 ± 0.58

Mice in
Sample with
Pathological
Kidneys
5

4

10

6

5

0

0
1

3

1

1


* C =  cortex;  (C)(M)  = cortex and medulla combined; DCT = distal convoluted tubule; DCT-I = inner  (straight)  region of distal convoluted tubule;
LH =  loop  of Henle; M =  medulla;  PCT = proximal  convoluted tubule;  PCT-I =  inner  (straight)  region of proximal  convoluted tubule; RC  =  renal
corpuscle.

t Hyperemia was estimated on a scale of 0 (none) to 5 (very marked).  Values are means ± SEM (n).

-------
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     Tetrazolium Reductases and Hydroxysteroid  Dehydrogenases  in  the  Gonads
     and  Adrenals  of  the Bank  Vole  (Clethrionomys glareolus):   Histochemical
     Study.  Biol. Reprod.,  21(1):125-133.
                                     273

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                                  SECTION 22
          SEASONAL CYCLES IN BODY COMPOSITION,  ORGAN SYSTEM FUNCTION
       AND ENERGETICS OF THE WESTERN MEADOWLARK IN SOUTHEASTERN MONTANA:
                             A REPORT OF PROGRESS
                    M.  L.  Morton,  R.  A.  Lewis  and E.  Zerba
                                   ABSTRACT

                 Results of a portion  of  a  baseline investigation
            of  grassland   birds   in  southeastern   Montana   are
            reported and  evaluated in relation  to  future  energy
            development.

                 Mensural  and compositional  characteristics  of the
            whole  body and  of  selected organs   of the western
            meadowlark   (_Stwcne11a neglecta}  are  treated.   The
            types  of systems  and functions  represented  are those
            that reflect the condition, vigor,  nutritional  state,
            metabolic  state and   resource  relationships  of  the
            study population.
                                    PREFACE

     This paper is a synopsis of a small portion of our baseline investigation
of  grassland  birds  in  southeastern  Montana in  relation  to  further  energy
development.   A monograph  is  in preparation that will more fully treat the
mensural and  compositional characteristics  of the whole body and of selected
organs of the western meadowlark (Sturnella negleata) and four  other species
of birds.  The monograph includes baseline  information on postnatal development,
reproductive  biology,  histology,  population dynamics and community structure.

     Results  reported herein  together with  those of the overall investigation
will permit evaluation of  the above aspects of avian organization as a func-
tion of age,  sex,  season,  and physiologic state in relation to  the physical
and biotic environment.  The  present analysis treats a number of types of
systems and functions that reflect the condition,  vigor, nutritional state,
resource relationships,  metabolic state, and net energy balance of the sample
                                      274

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population as a function of environmental information or gradients, including
potential changes  in  air quality and other anthropogenic disturbances related
to  future energy  development  in southeastern  Montana.   The  data  are essen-
tially baseline in nature.

     We believe  that future  air pollution  effects  research  in  the  northern
Great  Plains  will rely  heavily upon such results.  The work in its entirety
represents a baseline  evaluation of annual cycle and life cycle phenomena and
the mechanisms that  regulate  such functions  in  relation  to  potential vulner-
ability to air pollution induced stress.  See Lewis et al.  (1976), for a more
complete statement of objectives.
                                 INTRODUCTION

     During the first 3 years of the study  (1974-76) large numbers of avian
specimens were collected in Rosebud and Powder River Counties.  Previously we
reported preliminary information obtained on these specimens  (Lewis et al.,
1976, 1978).  The available data on western meadowlarks have now been consoli-
dated in the present report in order to characterize more fully the status of
this species in the southeastern Montana environment at a baseline or pre-
pollution condition.

     Data  on  bodily  composition  of  all  vertebrate  classes have  powerful
utility  as  measures of  condition, metabolic  and  energetic  stress,  and life
history strategies  (Connell et al., 1960; Helms, 1968; Helms and Smythe, 1969;
McNeil, 1969; Myrcha and Pinowski, 1970; Telford, 1970; Adolph and Hegeness, 1971;
Aleksiuk and Stewart, 1971; Perkins and Dahlberg, 1971; Krulin and Sealander,
1972; Morton et al. , 1974; Morton, 1975; Fehrenbacher' and Fleharty, 1976).

     Changes  in body  composition are also  adaptive and  highly predictable
measures  of age  and  phase  of  the  annual  cycle  (Morton, 1975;  1976).  Thus
deviations  from  normal  patterns  that  are  deleterious,   should  be  easily
detected  and  should  provide  strong   evidence  for presence  of environmental
perturbation.  Indeed, we  have  good  evidence  (Lewis et al • , unpublished data)
that  during certain phases  of the annual  cycle (e.Q->  reproduction, growth,
molt), that at least some of the  species under  investigation are living close
to  the limit  of their resources or are under  substantial environmental stress
that  may condition their responses to pollutants.  Special attention will be
given to these processes and their implications.  We hope eventually to deter-
mine  the extent  of pollution-related  effects  on small birds in the study area
and  to  distinguish, to  the  extent possible,  between  direct  and  indirect air
pollution effects  and  the  effects of  other human activities that might other-
wise  tend  to  confound  our results (e.g.,  effects of  coal-mining,  water use,
increased human population density, use of herbicides and pesticides,  eta.).

     Western meadowlarks  and other  grassland birds  are potentially valuable
monitors of environmental disturbance  because  they live  in  a relatively simple
environment wherein the effects  of  abiotic  factors  should  be  only slightly
buffered by the biotic community and thus easily discerned  (Weins, 1973; 1974).
This relationship has been amenable to development of useful models for energy
flow in grassland populations  (Wiens and Innis, 1974).

                                       275

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     The  annual  cycle  is  the  fundamental temporal  unit in most  long-lived
animals.  The essential processes  of  life such as winter maintenance,  migra-
tion, reproduction,  and molt  occur within a highly specific schedule such that
conflict between major  energy-requiring  events  and environmental fluctuations
and among the events themselves is minimized.   The precise duration and timing
of annually occurring  functions  are  therefore essential and comprise key loci
for  selection pressures that shape evolutionary  tendencies  toward  optimizing
an individual's fitness (Mewaldt and King, 1977).

     Some of  the organs  examined  in this  study,  vary appreciably  in  mass
during  the  season  (spleen,   liver,   gonads)  whereas  others   (heart,  lungs,
kidneys) do not.  Both  types  could have  considerable worth as pollution moni-
toring  systems.   For   example,  significant deviation  from normal  values  for
static  organs  could  be indicative  of  pathology.   Organs  that  cycle do  so
within highly specific temporal boundaries. Departure from the usual schedule
might be  a  harbinger  of environmental perturbation.  In  either case,  precise
diagnosis  of  pathology will  depend  upon corroboration through  additional
assessment of function.  Such  evaluations  would  logically involve biochemical
and  histochemical  characters  and  microstructural parameters such as cellular
size,  organization,   and  number.   Conducting evaluations  of  this  type  is
usually expensive in time and money.   Highly developed techniques and special-
ized equipment are also required.  Collection of organ weights, however,  is a
relatively straightforward  process that can be accomplished by any worker  with
simple equipment and basic  biological skills.   Changes in organ weights signal
qualitative or quantitative changes in organ structures and function and these
indicate bases for further analysis of tissues  that we have banked.


                             MATERIALS AND METHODS

     Specimens were  collected with a  shotgun,  sealed  in plastic  bags with  appro-
priate labels, and retained frozen until analysis.  In many specimens internal
organs were removed for weighing and/or  fixation.  In such cases, dissections
were performed at the  field vehicle immediately after shooting or the specimen
was placed on ice and  transported to  our  field laboratory at Fort Howes Ranger
Station, Powder River  County,  for dissection.  Collecting was done  in Rosebud
County along Rosebud,  Cow and Greenleaf Creeks within 15 km of Colstrip.  Some
specimens were collected in  Powder River County,  usually within 20  km of  Fort
Howes.

     In the laboratory  we  employed standard biometric methods  and  whole  car-
cass and  organ  analysis to  evaluate  compositional and mensural  changes  as a
function of age, sex,  season,  and physiologic state in relation to  the physi-
cal and biotic environment,  (for details,  see Lewis and Morton, 1976;  Lewis  et
al. , 1976, and below).

     Frozen specimens  were thawed and analyzed  as follows:

      1.  Molt classifications  were  determined by detailed observation,  the
          method  being  adapted  from  Morton et al ., (1969).  The just-thawed
          carcass was  then dissected and processed all or in part as follows:


                                      276

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      2.   Liver—wet weight, dry weight,  fat content, fat-free dry weight; to
          tissue bank.

      3.   Left kidney—wet weight, dry weight; to tissue bank.

      4.   Adrenals—wet weight,  return to carcass.

      5.   Thyroid—wet weight, return to carcass.

      6.   Gonads--wet  weight  of  testes,  ovaries  and  oviducts,  return  to
          carcass.

      7.   Spleen—wet weight, return to carcass.

      8.   Gizzard—wet weight, return to carcass.

      9.   Integument  (plumage)--dry  weight  (does  not  include  beak  or  leg
          scutes),  return to carcass.

     10.   Carcass—dry  weight   (wet  weight determined  in  field  on  date  of
          collection), dried tissue ground  and aliquots  used to determine fat
          content;  remainder to  tissue bank.
     Specific techniques used in making the measurements outlined above:

      1.  Wet weights of organs were made on a torsion balance as  soon as they
          were dissected free and blotted.

      2.  Grinding  of   carcasses  for production  of homogeneous  aliquots  was
          done in a Model 4-E Quaker City Laboratory mill.

      3.  Fat  content  was  determined by  placing  specimens  in  thimbles  and
          extracting them in a  soxhlet  apparatus with 1,2-dichloro-ethane for
          24 hours.  Samples were  then  dried at 75°C in  convection  ovens  and
          the fat-free  dry weight recorded.

      4.  Total nitrogen was  determined by  the  standard  micro-Kjeldahl  tech-
          nique .

      5.  Caloric content was measured  by combusting aliquots of  dried speci-
          mens in a Parr adiabatic calorimeter.

      6.  Mensural  techniques  on  plumage  and  appendages  were   adapted  from
          Baldwin et al-,  (1931).
                                    RESULTS

     The western meadowlark  is  monotypic  and considered to be  a  sibling spe-
cies of  the  eastern meadowlark,  S.  magna (Lanyon, 1962). It breeds  from the

                                     277

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Great Lakes region westward from Mexico to southern Canada.  Since the turn of
the  century,  in association with  settlement and deforestation  by man,  there
has been a  significant  extension of its range to the northeast (Lanyon,  1956).
This expansion is apparently still progressing (Rohwer, 1973).

     Meadowlarks may  range into mountain  parks and  foothills but are better
known as inhabitants  of  prairies and grassy plains.  They  winter in parts of
Mexico and  in southern  U.S.  border states but  have  been recorded as residing
the  whole winter as far north as Miles City, Montana  (Cameron, 1907). They may
begin arriving  in  Montana  on spring migration in late February or early March
(Weydemeyer, 1973), but an 18-year average first arrival time for Custer County
was  30 March  (Gross, 1958). Fall migration usually begins in October but a few
birds  are  known to  have departed  Montana  and  similar  latitudes as  late as
mid-November.

     The time  of  reproduction  is,  of course, the single  most critical period
in  any  organism's annual  cycle.   In the present study primary  evaluation of
this  period was made by the use  of weights of reproductive organs  used to
define the normal limits of gonadal development and the temporal limits of the
breeding period.
Gonads

     Our  collection  of  meadowlarks  began in early April when  the first indi-
viduals  arrived  in  the  study area.  Most  of  the birds  collected throughout
April were adult males, 126 of 145 or 87 percent.   Testes of males collected
in April were often one-third to one-half the size of those collected during
May and June (Table 22.1);  the size difference was highly significant (P <
0.01, t-test of means).  The first males to arrive quickly established and
began defending territories.  They were conspicuous because of  their frequent
bouts of singing from elevated perches.

     Females were not regularly present until May, at which time their ovaries
averaged more than 500 mg, significantly larger (P < 0.01) than those taken in
April  (Table 22.2).   In  both sexes, considerable  gonadal growth thus occurred
in many individuals after reaching the study area.

     Judging  from gonadal  and  oviduct  weights,  and  follicular  diameters,
adults of both  sexes typically maintained reproductive  function  until  mid or
late  July (Tables  22.1  and  22.2).   Gonadal  involution  in July  was  rapid,
spanning only a few weeks in the population that we sampled.

     A  few  fledglings were  present during  the  first half  of June  but they
could not be found  with  regularity until the last  half  of the month.   There
was no detectable  seasonal change in gonad  weights  of juveniles  (Tables 22.1
and 22.3).  Note that data  on meadowlark juveniles are presented according to
sex.   Differences in body size between the sexes were eventually evident to us
(see beyond), and the data were therefore segregated.

     In most avian species,  the  right ovary and oviduct do not persist beyond
early development, and ovarian  and oviduct weights  referred  to  here include
only those of the left side.  Oviduct size and functional status  is  primarily

                                      278

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TABLE 22.1.  SEASONAL CHANGES IN PAIRED TESTES WEIGHTS (mg) IN WESTERN
             MEADOWLARKS COLLECTED NEAR COLSTRIP, MONTANA, 1974-1978

Adults

April
May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
51
33
33
39
35
43
25
18
13
7
8
9
4
Mean
282.7
479.5
539.5
722.6
677.7
673.6
572.3
298.0
16.4
10.5
8.4
8.2
21.0
S.D.
139.2
189.7
152.3
146.8
176.6
183.3
220.0
257.5
7.1
4.4
1.4
3.2
20.2
N
--
--
2
12
8
14
11
29
34
23
6
Juveniles
Mean
--
--
4.8
3.6
3.9
6.7
8.0
5.2
4.3
3.6
4.0
S.D.
--
--
--
1.3
1.3
2.5
2.9
2.5
1.9
1.7
1.5

under  the  control  of ovarian hormones  although  it  does have independent vas-
cular  and  nerve supplies  (see  reviews by Lofts and Morton, 1973; Sturkie and
Mueller, 1976).  The  cycle  seen in  adult  female  meadowlarks  (Table  22.2),
therefore,  reflects  seasonal changes in secretion of ovarian hormones (estro-
gens and progesterone).  The diminutive size and lack of change in oviducts of
juveniles  indicates  that  their ovaries were  nonsecretory  from  June through
September (Table 22.3).

Body Weights and Body Composition

     Body weights  afford the most convenient standard  for comparisons of body
size  and  energetics  (Baldwin   and  Kendeigh, 1938).  Weights of meadowlarks
tended  to  decrease  during  the   season  and did  not  swing  upward until August
(Table 22.4).   Body  weights of  juveniles  increased  through  time  as  one would
expect  from normal  growth.   Both sexes  of  juveniles were approximately equiva-
lent to their adult counterparts  in body mass by September (Table 22.4).

                                       279

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TABLE 22.2.  SEASONAL CHANGES IN WEIGHTS (mg) OF REPRODUCTIVE ORGANS AND DIAMETER (mm) OF PRE-OVULATORY
             FOLLICLES IN ADULT WESTERN MEADOWLARKS COLLECTED NEAR COLSTRIP, MONTANA, 1974-1978.


April 1-15
16-30
May 1-15
16-31
June 1-15
to 16-30
oo
o
July 1-15
16-31
Aug. 1-15
16-31
Sept. 1-15
16-30
Oct. 1-15

N
1
12
35
33
22
15
15
13
6
9
10
5
1
Ovaries
Mean
81.10
107.78
560.00
537.79
414.65
519.35
108.97
42.05
15.05
13.45
20.04
21.36
10.91

S.D.
--
49.76
839.50
900.41
520.63
694.80
218.07
16.61
10.14
4.86
11.54
6.34
— —

N
1
13
35
32
21
17
17
12
5
8
9
3
1
Oviducts
Mean
357.90
275.23
1864.61
1575.46
1102.49
1319.94
356.02
128.14
57.08
40.36
51.55
22.41
23.54
Pre-ovulatory Follicles
S.D.
--
166.55
1824.54
1697.50
1412.55
1503.95
826.28
79.05
29.39
21.57
30.67
13.76
__
N Mean S.D.
__
58 2.22 0.55
141 3.53 2.28
140 3.45 2.53
63 3.68 2.99
63 3.86 2.91
19 3.60 3.21
6 1.08 0.48
—
__
__
__
	 	 	

-------
     No large seasonal  fluctuations  in measured body components were apparent
in adult  (Table 22.5)  or  juvenile (Table 22.6) meadowlarks, but  a  few trends
occurred.   Mean body weight,  for  example,  of adult males decreased during the
last half of  the  season.   This corresponded temporarily with postnuptial molt
(see beyond) but  the  possible physiological significance of this relationship
may be complex in that a similar trend did not occur in females.

TABLE 22.3.   SEASONAL CHANGES IN WEIGHTS (mg) OF REPRODUCTIVE ORGANS IN FEMALE
             JUVENILE WESTERN MEADOWLARKS COLLECTED NEAR COLSTRIP, MONTANA,
             1974-1978


June
July

Aug.

Sept.


16-20
1-15
16-31
1-15
16-31
1-15
16-30

N
11
8
7
8
16
19
15
Ovaries
Mean
3.11
5.04
5.71
3.90
3.53
5.06
8.06

S.D.
1.78
3.08
2.61
2.77
1.85
2.75
6.70

N
13
8
7
9
11
18
15
Oviducts
Mean
7.00
10.61
10.75
8.32
9.71
10.36
9.95

S.D.
2.85
1.57
1.63
2.47
6.41
5.79
4.28

     The nitrogen  content of  meadowlark carcasses  (Table 22.7)  and pectoral
muscle (Table 22.8) was  remarkably constant.

     Water   content   of  adult  males  tended  to   be   low   in  early  April
(Table 22.5).   Comparison of  the  early and  late  April means  indicates  that
they are marginally  different  (0.10 > P > 0.05).  This could be a real effect
because newly  arrived migrants are sometimes noticeably dehydrated (Zimmerman,
1965).   Rehydration  is  probably complete within the  first day  after arrival,
however, and one must be able to determine exact arrival schedules of indivi-
duals to have  confidence  in the carcass composition  data.  Unfortunately we do
not have precise information on arrival times  of  individuals.

     Apparently collections ceased before adults began premigratory fattening,
although the three males collected in October were fatter than birds collected
earlier (Table  22.5).  October samples of juveniles did not have significantly
more fat  than   those  of September  (P  < 0.05) when  all  data  on juveniles are
treated together.   Note that  sex  was  undetermined  in 42 juvenile specimens
but, because of its inherent value, data on their body composition is included
in Table 22.6).

                                      281

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     TABLE  22.4.   SEASONAL CHANGES IN BODY WEIGHTS (g) IN WESTERN MEADOWLARKS NEAR COLSTRIP, MONTANA
                  1974-1978
00
NJ

Adult Males

April
May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
76
50
46
46
42
51
28
29
22
12
12
12
3
Mean
118.67
116.61
113.66
114.70
112.93
110.56
110.54
110.89
115.21
118.53
116.79
118.88
131.70
S.D.
8.57
6.36
6.47
4.96
5.78
5.93
5.87
6.21
5.02
5.06
5.70
3.98
13.04
Adult Females
N
1
18
41
42
27
29
29
25
18
18
19
9
—
Mean
99.40
92.38
93.91
92.65
89.75
89.22
86.81
85.74
87.58
91.53
89.38
94.48
—
S.D.
6.56
6.76
8.99
6.67
9.61
5.69
5.96
6.77
5.29
4.59
3.61
—
Juvenile Males
N
--
--
2
14
15
33
31
46
44
33
11
Mean
--
--
69.67
87.83
94.28
98.89
104.23
107.33
110.34
115.21
121.366
S.D.
--
--
--
9.87
11.05
7.42
8.45
14.66
6.48
8.47
7.76
Juvenile Females
N
--
--
--
15
9
32
30
32
37
23
4
Mean S.D.
--
--
--
71.37
76.68
79.42
81.47
83.34
90.21
90.80
94.33
--
--
--
9.16
7.31
4.53
8.94
5.51
9.20
7.58
1.77

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TABLE 22.5.  SEASONAL CHANGES IN BODY COMPOSITION OF ADULT WESTERN
             MEADOWLARKS, 1974-1976

Water (% body weight) Lean (% body weight) Fat

MALES


April 1-15
16-30
May
June
July
Aug.
Sept.
Oct.
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
48
33
19
27
16
33
13
20
9
3
9
13
3
Mean
64.91
66.24
67.48
67.19
67.55
67.12
70.33
69.15
70.15
71.67
66.53
66.19
61.49
S.D.
6.31
1.87
1.89
2.52
1.96
1.62
3.64
3.13
2.15
2.15
11.68
3.47
2.85
N
46
30
18
25
16
21
12
20
6
3
9
12
3
Mean
29.44
28.66
28.58
27.96
28.09
28.14
24.97
26.17
25.11
24.05
25.92
27.54
27.97
3
2
1
2
1
1
3
2
3
2
4
3
1
S.D.
.17
.11
.52
.81
.99
.34
.16
.98
.10
.04
.88
.18
.27
N
46
30
18
24
16
31
12
20
6
3
9
12
3
(% body weight)
Mean S.D.
6.49
5.14
4.30
5.22
4.42
4.72
5.09
4.70
4.54
4.28
4.34
6.16
10.55
2.23
1.32
1.14
1.38
1.14
1.00
1.77
0.80
1.34
0.75
1.18
1.70
4.03
FEMALES
April
May
June
July
Aug.
Sept.
16-30
1-15
16-30
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
13
28
22
12
21
16
19
7
5
9
7
63.90
64.52
67.86
67.63
68.30
67.20
68.72
70.75
68.96
67.36
68.05
2.18
6.69
3.10
3.99
1.39
5.99
2.53
4.04
1.73
2.61
4.76
13
24
22
11
21
16
17
6
5
9
7
28.26
27.58
26.67
26.55
26.94
27.86
26.79
24.91
26.10
27.67
26.45
1
1
2
1
1
1
2
3
2
.12
.28
.53
.88
.31
.24
.31
.78
.90
2.01
23.48
13
24
22
11
21
16
17
6
5
9
7
8.08
6.78
4.82
5.46
4.82
5.01
4.46
3.94
4.93
5.28
5.73
2.08
2.30
0.93
0.86
0.93
0.84
1.32
0.90
1.40
2.30
2.41
                                      283

-------
TABLE 22.6.  SEASONAL CHANGES IN BODY COMPOSITION OF JUVENILE WESTERN
             MEADOWLARKS, 1974-1976


MALES
June
July
Aug.
Sept.
Oct.

f
1-15
16-30
1-15
16-30
1-15
16-31
1-15
16-30
1-15
Water
N
2
5
6
21
17
33
30
27
11
(% body
Mean
69.60
72.30
68.30
70.09
71.62
70.09
69.42
67.76
64.16
weight)
S.D.
1.78
9.48
3.17
2.65
1.92
2.66
2.48
3.35
Lean
N
2
5
6
21
14
29
29
24
11
(% body
Mean
22.72
23.85
27.46
24.92
23.54
25.46
26.81
26.92
27.46
weight)
S
2
9
2
2
1
1
1
1
.D.
.16
.52
.55
.18
.83
.99
.46
.47
Fat
N
2
5
6
21
14
29
29
24
11
(% body
Mean
7.69
3.92
4.24
4.91
4.64
4.31
4.08
4.95
8.38
weight)
S.D.
1.55
1.26
1.43
1.09
0.87
0.95
1.60
4.02
FEMALES
June
July
Aug.
Sept.
Oct.
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
4
13
13
21
25
19
3
70.13
70.44
70.63
70.41
68.64
67.60
62.76
1.49
1.16
3.57
2.43
2.32
1.46
2.81
4
12
12
18
23
18
3
24.80
23.49
24.33
24.78
26.38
27.30
26.71
1
5
3
1
1
1
1
.95
.27
.99
.62
.78
.31
.32
4
12
12
18
24
18
3
5.20
6.03
5.00
4.44
4.44
4.99
10.53
1.07
5.00
1.92
1.03
1.18
1.10
4.14
SEX UNDETERMINED
July
Aug.
Sept.
1-15
16-31
1-15
16-31
1-15
16-30
4
3
9
5
5
13
70.54
70.55
72.79
69.91
70.73
67.42
3.15
4.82
4.83
1.57
1.46
1.37
4
3
9
5
5
13
24.12
24.99
22.83
24.04
25.05
26.51
2
4
4
5
1
.38
.82
.10
.55
.72
.82
4
3
9
5
5
13
5.35
4.46
4.21
4.04
4.10
5.30
2.61
0.41
1.74
1.09
1.02
1.52
Oct.
1-15
                    64.77   3.06
                                   28.20   1.75
7.03   4.04
                                     284

-------
     TABLE  22.7.   SEASONAL CHANGES IN CARCASS NITROGEN (PERCENT DRY WEIGHT) IN WESTERN MEADOWLARKS,

                  1974-1976
to
00

Adult Males

April
May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
20
13
3
9
6
16
13
18
5
3
8
12
4
Mean
11.6
11.3
10.8
11.6
11.6
11.8
11.8
12.3
11.8
11.7
12.0
11.5
10.0
S
1
1
0
1
0
0
0
1
0
0
1
1
1
.D.
.0
.2
.5
.0
.7
.7
.7
.8
.7
.4
.0
.1
.5
Adult Females
N
3
10
5
8
14
13
9
6
1
9
4
--
Mean
10.6
11.4
11.7
11.5
11.6
11.7
12.1
11.7
11.6
11.5
10.4
—
S.D
1.
1.
1.
0.
1.
0.
0.
0.
--
1.
1.
--
•
1
0
1
9
2
9
7
3

6
6

Juvenile Males
N
--
--
1
4
4
16
6
19
27
21
7
Mean
—
--
11.9
11.7
11.7
12.4
11.5
12.2
12.0
12.1
10.8
S.D.
--
—
--
1.3
0.9
1.5
0.8
1.0
0.9
1.9
1.3
Juvenile Females
N
--
--
--
2
1
10
13
9
21
13
3
Mean
—
—
--
11.8
13.1
10.9
11.8
12.3
11.9
11.4
9.8
S.D.
--
—
--
--
--
1.6
0.8
1.6
0.8
1.3
2.2

-------
     TABLE 22.8.  SEASONAL CHANGES IN PECTORALIS NITROGEN (PERCENT DRY WEIGHT) IN WESTERN MEADOWLARKS,
                  1974-1976
00

Adult Males

April

May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
12
11
7
11
9
10
10
7
2
3
5
7
3
Mean
13.4
13.3
13.0
13.1
13.0
13.5
13.0
13.7
13.6
12.7
12.8
13.8
12.5
S.
0.
0.
0.
1.
0.
1.
0.
1.
--
0.
0.
0.
1.
D.
6
6
1
0
8
0
6
8

6
6
8
2
Adult Females
N
--
4
10
12
7
7
9
5
6
--
5
6
—
Mean
--
13.0
13.1
13.8
12.9
12.2
13.0
12.6
12.7
__
12.9
12.9
—
S.D
--
0.
0.
2.
0.
1.
0.
0.
0.
--
0.
0.
—
•

2
6
4
7
3
6
6
4

9
8

Juvenile Males Juvenile Females
N Mean
--
__
__
__
__
2 13.3
2 13.2
8 13.1
11 13.7
16 12.7
17 13.0
13 12.7
11 13.3
S.D. N Mean
__
__
__
__
__
1 20.4
1 12.8
0.5 6 12.8
1.1 8 12.8
0.8 16 12.9
0.8 24 13.6
0.7 10 13.2
0.6 3 12.8
S.D.
--
--
--
--
--
--
--
0.6
1.2
1.6
2.2
0.5
0.4

-------
     TABLE  22.9.   SEASONAL CHANGES IN CALORIES PER GRAM ASH-FREE DRY WEIGHT  (CARCASS AND  INTEGUMENT)  OF
                  WESTERN MEADOWLARKS, 1974


July
Aug.

Sept.

Adult Males
N Mean S.D.
16-31 1 4707
1-15
16-31 1 4783
1-15 1 4853
16-30
Adult Females
N
1
1
--
1
2
Mean S.D.
4865
4644
--
5335
4897
Juvenile Males
N
2
5
11
6
7
Mean
4845
4914
4851
4885
5010
S.D.
--
65
114
94
243
Juvenile Females
N
4
4
10
13
5
Mean
4922
4851
4865
5001
5015
S.D.
175
85
72
175
137
(~0
00

-------
     TABLE 22.10.  SEASONAL CHANGES IN LIVER WET WEIGHT  (mg)  IN WESTERN  MEADOWLARKS,  1974-1976
00

Adult Males

April

May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
44
31
14
18
12
26
9
17
5
5
10
13
3
Mean
2752.5
3051.4
2780.0
2689.0
2626.5
2733.4
2705.2
3218.3
2809.1
3572.9
3284.2
3313.8
3585.0
S.D.
691.4
346.6
458.8
349.0
438.6
343.6
450.7
570.4
436.5
947.4
422.8
536.6
780.3
Adult Females
N
--
12
26
16
9
16
7
16
5
5
10
6
—
Mean
--
2252.6
2681.1
2662.8
2611.1
2604.6
2580.8
2439.1
2361.9
3075.2
2551.4
2682.0
—
S.D.
--
285.7
610.3
519.4
488.1
472.8
366.2
369.8
210.5
386.0
284.9
296.6
—
Juvenile Males
N
--
--
--
--
2
5
4
9
13
30
36
27
12
Mean
--
--
--
--
1954.2
2640.2
3093.7
3022.1
3332.8
3284.7
3316.5
3522.4
3599.8
S.D.
--
--
--
--
--
315.5
388.9
611.9
393.9
620.8
511.7
627.4
948.1
Juvenile Females
N Mean
__
--
__
--
__
5 2222.2
1 2732.1
13 2724.0
11 2650.1
18 2635.3
28 2755.4
19 2789.6
2 2799.2
S.D.
--
--
--
--
--
300.2
--
426.0
377.8
221.8
479.4
266.7
— —

-------
     A  few  data  were  obtained  on  caloric  values  of  meadowlark  tissue
(Table 22.9).  These  values  were  fairly  consistent among  themselves  but,  in
general, they fell slightly below those reported previously for birds (Brisbin,
1968), Skar  et  al.,  1972).   Constancy in caloric value has  usually been found
in animal  tissues (Richman, 1958; Richman and  Slobodkin, 1960; Golley, 1961).
These data,  and  those of other species in this study, support the generaliza-
tion that nonfat components of migratory birds are fairly homeostatic consider-
ing  the  great seasonal  swings that  occur  in  their  energy expenditures  (see
Odum et  al.,  1965).

Liver

     Weights  and chemical composition  of livers  were measured  in nearly 600
meadowlarks (Tables 22.10- 22.14). Livers of adult males tended to enlarge
TABLE 22.11.
SEASONAL CHANGES IN LIVER COMPOSITION OF ADULT WESTERN
MEADOWLARKS, 1974-1976

Water % liver weight)

Males
April

May

June

July

Aug.

Sept.

Oct.


1-15
16-30
1-15
16-31
1-15
16-30
" -15
1 31
1-15
16-31
1-15
16-30
1-15
N

42
26
14
17
12
26
9
17
6
5
10
12
3
Mean

70.40
71.59
70.08
70.51
69.69
70.78
70.26
71.86
71.72
71.59
71.93
70.31
68.63
S

2
4
1
1
1
2
1
1
1
1
0
1
0
.D.

.42
.40
.59
.58
.07
.06
.98
.44
.74
.49
.88
.49
.57
Lean
N

42
25
14
17
12
26
9
14
4
4
8
11
3
(% liver weight)
Mean

24.67
24.31
25.86
25.53
25.29
24.32
24.57
24.47
23.69
24.67
24.46
24.58
25.55
S.D.

2.61
4.06
1.24
1.22
2.83
1.35
2.22
1.33
1.75
2.32
0.85
1.07
2.52
Fat (% liver
' N

42
25
14
17
12
26
9
14
4
4
8
11
3
Mean

4.95
4.14
4.06
3.96
4.40
4.90
5.17
3.59
4.21
3.88
3.83
5.07
5.83
weight)
S.D.

2.05
1.41
1.10
0.69
1.05
1.53
0.69
0.72
1.05
0.68
1.01
1.48
2.80
Females
April
May

June

July

Aug.

Sept.

16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
11
22
16
9
15
9
16
5
5
10
8
70.35
70.28
70.40
71.52
71.51
70.85
72.07
71.94
71.70
71.06
69.82
1
2
1
2
2
2
2
1
1
1
1
.49
.20
.72
.55
.17
.26
.13
.82
.72
.40
.74
11
21
16
9
13
9
16
4
5
9
8
25.32
25.03
24.85
23.42
23.02
24.45
23.56
24.03
24.14
24.88
25.12
1.39
1.36
2.67
2.45
2.87
1.69
2.21
1.66
1.13
1.00
1.43
11
21
16
9
13
9
16
4
5
9
8
4.34
5.09
4.96
5.06
5.28
4.81
4.37
4.10
4.16
4.31
5.46
0.45
1.39
1.31
0.68
1.25
1.30
1.10
1.31
1.68
0.84
1.69
                                      289

-------
TABLE 22.12.
SEASONAL CHANGES IN LIVER COMPOSITION OF JUVENILE WESTERN
MEADOWLARKS, 1974-1976

Males
June

July

Aug.

Sept.

Oct.


1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
Water
N

2
5
4
17
13
30
36
27
11
% liver
Mean

73.27
71.34
72.27
72.69
72.71
72.06
71.56
69.79
68.53
weight)
S.D.

— _
1.26
0.19
1.31
2.03
1.29
1.66
2.87
2.19
Lean
N

2
5
4
16
11
28
34
25
11
(% liver
Mean

23.27
23.88
23.62
23.72
24.11
24.39
24.36
25.32
25.12
weight)
S.D.

	
1.73
1.22
1.36
1.62
1.53
1.39
1.58
1.79
Fat (%
N

2
5
4
16
11
28
34
25
11
liver
Mean

3.46
4.78
4.12
3.64
3.73
3.56
4.03
5.06
6.16
weight)
S.D.

—
0.58
1.05
0.80
0.81
0.98
0.86
2.21
3.36
Females
June
July

Aug.

Sept.

Oct.
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
5
1
14
11
18
28
19
3
70.12
73.54
72.36
71.85
71.44
71.06
70.22
70.72
0.79
—
1.15
1.92
1.46
1.67
2.08
0.58
5
--
13
9
17
28
18
2
23.23
21.46
23.40
24.85
25.23
24.84
25.13
25.18
3.11
--
1.03
1.46
1.30
1.44
1.47
— —
5
1
13
9
17
28
18
2
6.64
5.04
4.26
3.69
3.31
4.11
4.71
4.43
2.94
--
1.00
1.09
0.58
0.96
1.68
— —

during the  last  two  months  of the collection period (Table 22.8).  These were
matched  in  size  by  those  of juvenile  males.   This change  in liver  size  of
males was unmatched by seasonal alterations in liver composition; the reported
components  of  the  liver remained  remarkably constant  in terms  of relative
proportions.

     Because of  its  central  role in intermediary metabolism,  especially as a
storage  site for nutrients,  the  liver may vary considerably in mass according
to diet,  feeding habits,  and energy expenditures (Oakeson, 1953; Hanson, 1962;
Pendergast and Boag,  1973;  Ankney, 1977).

     Of  pertinence to  the present study, seasonal  changes  in liver mass have
been noted  in  migrants  in  that they decrease  sharply  during spring migration
(Oakeson, 1953).  Liver  weight may also  decrease  during  incubation especially
in species,  such as  geese,  that exhibit reduced rates  of feeding at that time
(Ankney, 1977).
                                      290

-------
    TABLE 22.13.  SEASONAL  CHANGES  IN LIVER DRY  LIPID  INDEX  (FAT AS PERCENT  DRY  WEIGHT)  IN WESTERN
                  MEADOWLARKS,  1974-1976
K3

Adult Males

April

May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
48
27
17
26
13
31
12
15
5
4
8
11
3
Mean
20.32
19.19
15.57
14.60
16.91
19.61
20.97
15.17
17.90
16.03
15.75
20.63
23.71
S.D.
12.56
8.18
4.58
3.15
4.70
6.36
4.52
4.12
4.13
4.08
4.60
6.45
14.04
Adult Females
N
--
11
23
18
3
15
10
20
6
5
9
7
__
Mean
--
17.44
20.45
18.65
21.68
27.91
22.17
18.78
18.46
17.34
17.38
22.09
—
S.D.
--
1.83
6.03
5.11
6.13
16.61
7.54
6.64
5.12
7.11
3.58
7.63
—
Juvenile Males
N
--
--
--
--
2
5
5
19
14
29
34
24
10
Mean
--
--
--
--
15.22
20.27
18.00
16.93
16.32
14.69
16.43
20.10
25.32
S.D.
--
--
--
--
--
4.07
4.84
5.14
3.90
4.59
3.79
8.17
18.10
Juvenile Females
N Mean
__
__
__
__
__
5 30.66
8 18.73
8 18.21
12 14.35
21 14.68
25 17.07
12 17.98
3 23.16
S.D.
--
--
--
—
—
19.59
5.35
5.50
2.75
4.03
6.05
5.24
9.64

-------
     TABLE  22.14.   SEASONAL CHANGES IN LIVER NITROGEN (PERCENT DRY WEIGHT) IN WESTERN MEADOWLARKS,  1974-1976
NO

Adult Males

April

May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
12
18
5
4
1
6
6
5
8
3
5
7
1
Mean
13.0
12.9
12.7
12.7
12.6
12.8
12.7
12.5
13.0
12.5
13.0
12.9
11.0
S.D.
0.6
0.6
0.5
0.4
--
0.4
0.5
0.6
0.8
0.3
0.6
0.7
—
Adult
N
--
6
8
3
2
5
7
9
3
4
5
4
—
Females
Mean
--
13
13
12
12
12
12
12
12
13
12
13
_

.0
.1
.7
.6
.9
.9
.9
.6
.1
.5
.1
_
S
-
0
0
0
-
0
0
0
0
1
0
0
_
.D.
-
.8
.3
.4
-
.4
.2
.7
.5
.1
.3
.5
_
Juvenile Males
N Mean S.D.
__
--
--
__
--
1 11.8
1 13.4
11 12.7 1.0
7 12.7 0.4
13 13.0 0.6
25 13.1 0.7
10 13.0 0.6
5 12.5 0.7
Juvenile Females
N Mean S.D.
__
__
__
—
__
1 12.9
1 12.7
4 13.5 0.7
4 12.5 0.2
7 13.3 0.5
10 13.0 0.7
5 13.0 0.3
2 11.8

-------
Other Organs

     Other  organs  of meadowlarks  that were  weighed routinely included heart
(Table 22.15),  lungs  (Table 22.16),  spleen   (Table 22.17),  adrenal  glands
(Table 22.18),  thyroid  glands  (Table  22.19),  and  left  kidney (Table 22.20).
One kidney  was  weighed  because there  is  no weight asymmetry between left and
right kidneys  in  birds  (Johnson, 1968).  Kidneys were also examined for nitro-
gen content  (Table 22.21).  Spleens tended  to become much larger as the season
progressed.  Spleens  in  September  were,  for example, nearly twice as large as
those of  April  in both adult sexes, a difference that was significant in both
cases (P  <  0.05).   This  is at least partly related to increased production of
blood (and perhaps immune bodies) during molt.

     The highly practical aspects of understanding  cardiac function has led to
its intensive  study  in  a  wide  range  of higher  animals.   In birds  a  rather
complete  review of heart anatomy and physiology has been completed by Sturkie
(1976) .    Heart  weights  have been  reported  for  many avian  species  (Hartman,
1955; Brush, 1966),   There seems to be a predictable, but allometric relation-
ship  between  heart  size  and  body size.   Hearts are  relatively larger  in
smaller birds.  In birds of the approximate size utilized in the present study
the heart would be  expected  to  comprise 1 percent or more of body weight.
Environmental factors,  such  as  high altitude,  are  known to  affect heart size
in birds  (see review by Carey and Morton, 1976), but regular seasonal oscilla-
tions are unreported.  An  apparent decrease  of  heart  weight  throughout  the
breeding season in adult female meadowlarks is not  readily explanable by us.

     Splenic function has been poorly studied in birds,  especially wild birds.
However, it is known  to receive about 3-4 percent of cardiac output in chickens
(Sapirstein and Hartman, 1959).  And it may vary seasonally in mass in both
sedentary (Riddle, 1928b) and migratory (Oakeson,  1953) birds.   We find no
reported data on breeding birds that can be used for comparative purposes with
our data.

     Size of  adrenal glands  varies with  species,  sex,  age,  health and a host
of  factors  related  to  physical stress such  as temperature,  disease, vitamin
deficiency,  and exercise  (see review by Ringer, 1976a).  Daily  and  seasonal
rhythmicities in function  are  known  to  occur, particularly  in  relation  to
photocycle.  Measurement  of  these functions  cannot be  determined reliably  by
whole gland  weight;  plasma or urinary corticosteroid titers are required (see
review by Assenmacher, 1973).  Cytologic  changes  occur  seasonally in adrenals
of  migratory  birds   (Burger,  1938; Fromme-Bouman,  1962; Lorenzen  and   Farner,
1964).

     The avian thyroid is paired and lobes  are  located in the neck next to the
great blood  vessels. As  in  mammals,  the gland is  involved in a wide range of
functions such as growth, heat production,  carbohydrate  metabolism, and sexual
maturation.   It  also  affects migratory  behavior  and  onset  of molt  in some
birds and growth of young feathers (Assenmacher, 1973).
                                      293

-------
TABLE 22.15.  SEASONAL CHANGES IN HEART WET WEIGHT (mg) IN WESTERN MEADOWLARKS, 1974-1976

Adult Males

April

May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
50
26
13
20
14
29
11
18
7
3
10
13
3
Mean
1560.03
1604.48
1575.75
1537.21
1393.93
1422.66
1397.69
1381.65
1311.71
1262.97
1372.38
1408.00
1793.30
S.D.
287.80
180.23
204.36
137.63
138.43
189.06
197.66
224.40
157.49
82.15
197.86
346.78
320.03
Adult Females
N
--
12
25
17
8
14
12
19
5
5
10
8
—
Mean
--
1257.81
1198.23
1132.81
1020.63
1030.04
1035.21
977.65
976.44
999.94
975.02
1067.71
—
S.D.
--
103.50
163.03
147.89
80.08
194.29
91.50
315.30
118.04
158.75
110.40
127.30
—
Juvenile Males
N
—
--
--
--
2
6
4
20
17
32
34
27
10
Mean
--
—
--
—
749.20
786.10
1176.94
1138.90
1169.20
1131.30
1224.40
1290.20
1383.10
S.D.
--
--
--
—
--
176.90
390.60
298.40
153.40
141.00
171.90
151.30
77.70
Juvenile Females
N Mean
__
--
__
__
__
5 773.40
1 723.00
13 957.20
13 877.10
18 898.50
24 972.43
19 1017.30
2 1053.90
S.D.
--
--
--
--
--
150.50
--
146.90
168.30
131.10
148.80
117.30
—

-------
TABLE 22.16.  SEASONAL CHANGES IN WET WEIGHT (mg) OF BOTH LUNGS IN WESTERN MEADOWLARKS, 1974-1976

Adult Males

April
May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1=15
16-30
1-15
N
31
19
6
13
8
19
7
13
4
4
8
12
3
Mean
1678.7
1663.4
1801.0
1601.8
1516.7
1584.9
1670.2
1786.5
1551.4
1689.4
1585.3
1501.6
1621.4
S.D.
224.0
227.1
325.3
180.2
246.9
214.1
289.5
316.1
249.9
165.9
105.3
261.1
286.6
Adult Females
N
8
20
14
8
11
11
13
4
4
7
5
—
Mean
1351.7
1227.8
1265.3
1198.7
1154.1
1131.0
1254.9
1122.8
1245.4
1157.5
1158.4
__
S.D.
142
143
172
205
238
182
191
64
222
119
118
—

.1
.0
.6
.0
.8
.7
.2
.0
.7
.3
.6

Juvenile Males
N
--
--
1
3
2
17
12
27
29
24
8
Mean
--
--
928.4
1096.8
1555.9
1415.0
1381.8
1435.0
1419.5
1453.9
1453.2
S.D.
--
--
--
313.1
--
196.0
179.0
190.5
196.2
225.3
330.4
Juvenile
N
--
--
--
3
1
11
11
18
21
17
3
Females
Mean
--
--
--
1013
937
1298
1046
1147
1127
1074
1064



.4
.9
.7
.6
.6
.2
.0
.7
S.D.
--
--
--
145.0
--
617.1
151.7
453.8
215.1
156.2
30.4

-------
TABLE 22.17.  SEASONAL CHANGES IN SPLEEN WET WEIGHT (mg) IN WESTERN MEADOWLARKS, 1974-1976

Adult Males

April 1-15
16-30
May 1-15
16-31
June 1-15
16-30
NJ
S July 1-15
16-31
Aug. 1-15
16-31
Sept. 1-15
16-30
Oct. 1-15
N
47
29
36
32
30
41
20
21
16
6
7
11
1
Mean
141.7
121.0
130.3
174.7
120.8
180.8
180.0
243.4
268.8
446.1
235.7
287.5
164.9
S.D.
111.1
94.3
86.2
209.6
100.8
131.0
167.0
121.1
238.5
467.9
130.2
165.3
—
Adult Females
N
1
14
28
30
22
13
17
18
9
9
10
8
0
Mean
109.4
137.1
152.1
136.9
117.2
141.5
141.8
152.8
134.5
173.1
191.5
221.7
—
S.D.
--
104
128
98
74
81
105
101
86
103
67
100
—


.0
.0
.7
.7
.1
.0
.3
.8
.4
.6
.0

Juvenile Males
N Mean
__
__
__
__
__
13 129.5
15 70.3
25 130.3
18 218.2
25 182.8
28 178.6
24 140.7
11 201.7
S.D.
--
--
—
--
--
126.6
31.2
104.2
208.3
199.3
175.8
85.5
115.5
Juvenile Females
N Mean
__
__
__
--
__
16 77.9
8 70.0
31 178.9
11 193.7
14 156.8
25 138. 5
19 178.7
4 162.6
S.D.
—
--
--
--
--
34.8
29.2
254.1
198.0
158.6
71.6
138.9
102.3

-------
     TABLE 22.18.   SEASONAL CHANGES IN WET WEIGHTS (mg) OF PAIRED ADRENAL GLANDS  IN WESTERN MEADOWLARKS,
                   1974-1978
I-O
VO

Adult

April
May
June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
34
23
31
28
34
43
20
19
10
5
8
10
1
Males
Mean
7
7
6
6
7
6
7
6
6
6
6
7
7
.2
.6
.2
.3
.1
.7
,0
.8
.9
.0
.3
.4
.9
S.D.
2.8
3.4
2.1
2.4
3.1
2.8
2.7
2.1
1.6
1.6
3.0
1.7
—
Adult
N
9
27
24
21
13
19
18
10
6
6
8
—
Females
Mean
5
6
6
6
7
6
5
6
5
7
8
_
.9
.4
.0
.5
.1
.4
.1
.9
.3
.0
.9
_
S
2
3
2
2
3
2
2
2
1
2
3

.D.
.9
.3
.6
.7
.4
.0
.0
.9
.3
.4
.5
__
Juvenile Males
N
--
1
11
12
27
15
26
32
21
8
Mean
-
7
7
6
6
6
5
7
8
7
-
.2
.1
.2
.9
.9
.9
.3
.0
.8
S
-
-
2
3
2
2
2
3
2
2
.D.
-
-
.1
.2
.2
.8
.3
.0
.4
.1
Juvenile Females
N
--
--
16
8
31
14
15
19
15
3
Mean
-
-
5
4
6
5
5
7
6
9
-
-
.7
.3
.0
.7
.6
.3
.2
.3
S.D.
—
--
2.4
2.0
2.9
1.9
1.5
3.1
2.1
2.9

-------
     TABLE  22.19.   SEASONAL CHANGES IN WET WEIGHTS (rag) OF PAIRED THYROID GLANDS IN WESTERN MEADOWLARKS,
                   1974-1978
00

Adult Males

April
May
June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
39
23
33
29
30
40
17
19
14
5
5
5
—
Mean
6.4
6.1
6.3
8.5
7.4
9.7
8.7
8.8
8.4
8.2
7.0
8.5
—
S.D.
2.6
2.0
2.7
3.6
3.1
4.8
3.8
3.1
2.9
3.4
3.4
3.5
—
Adult Females
N
1
7
23
16
18
16
18
18
8
10
4
2
—
Mean
5.0
7.3
8.1
8.5
8.0
8.5
6.6
7.3
7.5
5.7
7.7
3.3
—
S.D.
2.3
6.2
4.3
4.8
4.3
3.9
3.1
2.2
2.2
2.7
--
—
Juvenile Males
N
--
2
12
13
23
10
14
21
11
—
Mean
--
11.7
8.4
5.2
7.6
6.9
7.7
8.2
8.3
	
S.D.
--
--
4.4
1.4
2.9
2.2
2.3
2.0
2.2
	
Juvenile Females
N
--
--
15
7
25
6
5
8
5
1
Mean
--
--
7.3
5.2
5.3
7.3
5.8
7.7
8.7
11.6
S.D.
--
--
4.8
1.3
2.1
2.7
1.2
3.2
2.2
_ _

-------
TABLE 22.20.  SEASONAL CHANGES IN WET WEIGHTS (rag) OF LEFT KIDNEY IN WESTERN MEADOWLARKS, 1974-1976

Adult Males

April

May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
29
17
9
16
11
26
7
15
5
3
9
7
3
Mean
385.5
502.9
478.4
471.6
464.3
487.5
479-2
569.8
546.8
595.9
592.6
517.6
617.8
S.D.
127.7
58.3
45.6
43.2
61.6
54.9
68.9
99.0
50.4
77.3
63.5
69.0
90.7
Adult Females
N
--
10
22
18
9
13
7
13
4
4
8
7
—
Mean
--
434.7
460.6
443.9
424.4
449.9
458.0
437.2
409.2
541.6
463.0
468.1
—
S.D.
--
43.5
85.2
55.8
70.0
45.9
46.4
51.2
52.7
101.5
49.3
60.6
—
Juvenile Males
N
--
--
--
--
1
5
5
15
10
28
33
25
10
Mean
--
--
--
--
343.3
409.1
385.2
500.2
471.4
478.8
542.9
512.2
603.8
S.D.
--
--
--
--
--
66.4
40.8
79.7
109.9
133.6
86.3
86.9
47.3
Juvenile Females
N Mean
--
__
__
__
__
2 377.0
1 282.6
11 423.8
11 415.8
18 419.7
22 449 . 1
17 464.3
2 464.7
S.D.
--
--
--
--
--
--
--
57.8
63-6
80.8
57.8
41.5
	

-------
     TABLE 22.21.   SEASONAL CHANGES IN KIDNEY NITROGEN (PERCENT DRY WEIGHT) IN WESTERN MEADOWLARKS, 1976
o
o

Adult Males

April

May

June

July

Aug.

Sept.


1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
N
13
6
4
9
7
17
4
11
5
1
3
2
Mean
12.3
12.5
12.3
12.3
12.0
12.3
12.4
12.4
12.5
13-9
13.6
15.6
S.
9.
1.
2.
4.
2.
5.
0.
4.
7.
--
4.
--
D.
3
9
2
2
4
5
8
8
7

2

Adult Females
N
--
4
8
4
5
9
4
8
1
4
3
_-
Mean
--
12.4
12.3
12.4
12.2
12.0
12.1
12.7
11.8
13.9
13.1
--
S
-
5
10
6
5
1
1
14
--
6
1
-
.D.
-
.2
.4
.0
.1
.7
.0
.5

.5
.5
-
Juvenile Males Juvenile Females
N
--
--
--
--
1
3
3
11
3
13
4
6
Mean S.D. N Mean S.D.
--
__
__
__
12.0
11.8 0.6 2 12.5
12.0 0.6
12.4 3.9 5 12.3 4.3
12.4 2.5 2 13.9
13.9 13.1 2 13.3
14. 2 15.3 3 14.1 18.2
15.1 16.3 4 16.1 21.75

-------
    TABLE 22.22.   SEASONAL  CHANGES  IN DIAMETER (mm)  OF  LARGEST THYMUS  LOBE IN WESTERN MEADOWLARKS,  1974-1975
u>
o

Adult Males

April

May

June

July

Aug.

Sept.


1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
N
22
15
7
11
9
8
5
6
1
3
4
5
Mean
0.4
2.5
3.0
3.6
3.6
3.9
5.3
4.4
4.4
6.7
5.9
5.7
S
0
1
0
0
1
1
1
1
-
1
2
1
.D.
.8
.2
.7
.7
.1
.0
.6
.3
-
.4
.8
.1
Adult
N
--
6
14
14
7
8
6
5
4
--
4
4
Females
Mean
--
2.
3.
3.
4.
3.
4.
4.
4.
--
5.
5.

8
5
8
1
6
1
1
8

1
6
S.
--
0.
0.
0.
1.
1.
1.
1.
1.
--
0.
1.
D.

9
9
6
2
4
6
1
7

5
2
Juvenile Males Juvenile Females
N Mean S.D. N Mean S.D.
__
__
__
—
__
1 6.8 — I 4.2
2 5.5 -- I 4.6
6 5.5 1.2 6 6.1 1.3
9 5.7 1.4 5 6.0 1.5
15 5.6 1.1 14 5.9 1.1
14 5.3 0.7 18 5.0 1.2
12 5.2 1.2 10 5.0 0.8

-------
     Weight of  thyroid glands  varies  seasonally, being  largest  in winter in
most,  (see Miller, 1939;  Wilson and Parner, 1960), but not all, species.
Increased size  can  be  a function of both  cell  size or number (see reviews by
Hohn, 1950 and Ringer,  1976b).  Thyroid (and  adrenal)  weights  sometimes vary
inexplicably  in wild  birds  (Hartman, 1946).   Some  of  this  variance  may be
related to  shifts  in  diet(Riddle and Fisher, 1926) as well as in temperature.
There  is,  however, a  general positive correlation  of both  glands with body
size   (Hartman  and  Brownell,  1961).    And   within a  given species,  seasonal
changes  in weight of  thyroids  may  serve  as  a useful  index  to secretory
activity  (Kendeigh  and  Wallin, 1966).  The perspective provided by histological
examination is  necessary  to understand functional condition  of  thyroids at a
given time;  weights alone are unsatisfactory for this purpose.

TABLE 22.23.  SEASONAL CHANGES IN WET WEIGHT (mg) OF BURSA OF FABRICIUS IN
              JUVENILE WESTERN MEADOWLARKS, 1974-1976

Males

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
1
16
14
30
21
33
34
24
10
Mean
51
99
98
170
173
186
196
192
160

.5
.5
.8
.1
.4
.1
.2
.2
.6
S.D
--
34
34
71
63
54
72
60
47
•

.1
.8
.0
.9
.7
.2
.3
.4
N
--
14
7
29
14
18
24
19
2
Females
Mean
--
83
121
152
156
171
170
158
169


.8
.7
.6
.1
.2
.8
.6
.7
S.D
--
36
41
66
76
29
60
39
__


.1
.0
.0
.7
.5
.5
.5


     The  kidneys  of  birds are symmetrically paired structures located in bony
 depressions  of  the  fused pelvis.  They usually comprise  about 1 percent of
 the  body weight  in  birds.   Their relationship to  body weight is allometric,
 however,  and they are relatively larger in small birds and in some desert and
 marine  types.  The kidneys through osmoregulatory controls, maintain water and
 electrolyte balance (see review by Shoemaker, 1972).

     Data  were  also gathered on  the  diameter  of the  largest  thymus lobe
 (Table  22.22),  weight  of the bursa  of Fabricius  (Table 22.23),  and gizzard
 weight  (Table 22.24). The bursa of Fabricius is a  dorsal diverticulum of the
                                      302

-------
    TABLE 22.24.   SEASONAL  CHANGES  IN EMPTY GIZZARD  WET WEIGHT (mg)  IN WESTERN MEADOWLARK,  1974-1976
o
Co

Adult Males

April

May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
N
47
29
17
24
16
34
15
21
8
5
10
11
3
Mean
2945.6
2403.3
2145.5
1957.9
1803.1
1867.8
1845.9
2021.7
2353.8
2716.1
2720.2
3135.8
3453.5
S.D.
390.5
471.9
222.1
306.9
330.9
382.8
220.6
406.8
243.4
285.2
221.4
369.9
216.4
Adult Females
N
--
11
26
20
14
21
11
17
8
5
10
7
—
Mean
--
1010.9
1811.6
1817.5
1707.5
1548.6
1520.6
1608.8
1839.7
2265.8
2283.4
2411.4
—
S.D.
--
207.1
238.0
237.4
218.0
179.4
154.6
203.9
354.0
326.8
146.1
192.2
—
Juvenile Males
N
--
--
--
--
1
5
5
20
16
32
35
27
11
Mean S.D.
__
__
__
__
1955.6
1726.8 273.1.
1746.0 379.5
1984.8 212.6
2512.6 316.2
2700.6 386.0
2908.3 459.8
3060.6 303.7
3140.3 266.4
Juvenile Females
N
--
--
--
--
--
5
1
13
12
18
26
18
1
Mean
--
—
--
—
--
1459.4
1465.2
1828.1
1969.6
2200.0
2424.8
2548.1
2774.7
S.D.
—
--
—
--
--
127.9
--
178.0
292.0
194.8
319.0
279.9
	

-------
proctodeal region of  the  cloaca.   Its major functions  include the regulation
of humoral antibody production (Click, 1964; Chang et al,, 1957; Warner and
Szenberg, 1964; Cooper et al.,  1967).  The secretion of a diffusible factor
which acts on lymphoid tissue (Click, 1960a; Jankovich and Leskovitz, 1965; St.
Pierre and Ackermann 1965), and the synthesis of immunoglobulins (Grossi et al.j
1968; Thornbecke et al.,  1968;  Zaccheo et al.,  1968; Click, 1977).  Basically
it contributes to immunological competence.

     The bursa is restricted  to  birds,  being largest in young birds and tend-
ing to involute  with  advancing age.   Maximum size is reached during the first
few weeks  of life,  but  the exact time varies among species,  being about 69
days in the pigeon (Riddle, 1928a), 110 days in;he pheasant (Kirkpatrick 1944)
and 56  days  in  the mallard (Johnson 1961).  After the  bursa obtains maximum
size it  involutes and eventually  disappears (Jolly, 1913; Schauder, 1923, Click,
1960b; Ward and Middleton, 1971).

     Both the thymus and  the bursa of the western meadowlark persist for an as
yet  undefined  period   following the  assumption  of  the  winter  plumage.   This
allows us  to easily  distinguish  adult  birds  and birds of the  year at least
throughout the  fall.

     The  bursa   is   necessary  for  the   development   of  antibody-mediated
responses.  It normally  involutes when a bird  reaches  sexual maturity.  How-
ever, it will involute earlier if the younger bird is subjected to stress.  It
will, for example, regress in the presence  of glucocorticoids (see Lewis  et
al. , 1976).   Consequently,  it should  be  very useful  for  identifying stressors
of young birds.  Sudden regressive changes in the structure  of the bursa are
more  likely  to  be  translated  quickly into  histological  changes  than  into
reductions in the weight of the gland.

     The thymus gland  is  an elongate  structure, usually with seven lobes,  that
lies  laterally  in the mid-  and   lower  neck.   The avian  thymus,  like that of
mammals,   is  involved  in  immunological processes, including  lymphocyte forma-
tion.  Along  with the bursa  it  is  thought  to  comprise a  dual  immunologic
system in  birds.  Both organs direct the  maturation of immunologically  com-
petent cells  capable of reacting to antigens (Assenmacher, 1973).

     In  all  vertebrates  the thymus  typically increases  in  size until sexual
maturity and then regresses  markedly.   In birds, however, the  process  can be
reversed and the gland may enlarge again  following  reproduction (Hohn,  1956).
This was observed in meadowlarks  in that juveniles had relatively large glands
whereas  those  of adults  were  small  during the first half of  the  summer  (the
period of reproduction) and tended to  enlarge thereafter  (Table  22.22).

     The gizzard or stomach of seed-eating birds characteristically is highly
muscular  in  keeping  with  its  function as  the site where  food is pulverized
before passage  to the main digestive and  absorptive portions  of  the gastro-
intestinal tract.  In this capacity it is, of course, the functional analog of
teeth in birds.  It may  also  serve as a chamber for food storage and for acid
proteolysis (Ziswiler  and  Farner,  1972).

     Seasonal  changes  in  gizzard  size  are to  be anticipated  as  a result of
dietary changes;  both  due to food  choice  or to quantity of intake. Reduced

                                     304

-------
     TABLE 22.25.   PERCENT OF WESTERN MEADOWLARKS SHOWING MOLT, 1974-1977
o
Ln

Adult Males
Number
N in molt
April
May

June

July

Aug.

Sept.

Oct.
1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15
76
49
47
46
42
51
27
28
14
7
12
14
3
0
0
0
0
0
1
11
23
13
5
12
13
1
Percent
molting
--
--
--
1.96
40.74
82.14
92.86
71.43
100.00
92.85
33.33
Adult
Nunber
N in molt
1
15
45
36
26
29
28
24
12
13
17
8
—
0
0
0
0
0
0
5
10
9
13
16
7
--
Females
Juvenile Males
Percent Number
molting N in molt
--
2
2
8
17.86 19
41.67 30
75.00 33
100.00 45
94.12 52
87.50 28
11
--
0
0
1
7
23
28
44
52
25
9
Percent
molting
--
0
0
12.50
36.84
76.67
84.85
97.78
100.00
89.29
81.82
Juvenile Female
Number
N in molt
--
--
1
8
7
33
25
44
38
22
3
--
--
0
2
5
17
23
31
36
22
2
Percent
molting
—
--
0
25.00
71.43
51.52
92.00
70.45
94.74
100.00
66.67

-------
     TABLE 22.26.  SEASONAL CHANGES OF INTEGUMENT DRY WEIGHT (rag) IN WESTERN MEADOWLARKS, 1974-1977
CT\


April
May

June

July

Aug.

Sept.

Oct.

1-15
16-30
1-15
16-31
1-15
16-30
1-15
16-31
1-15
16-31
1-15
16-30
1-15

N
49
35
19
27
17
34
16
22
8
4
10
12
3
Adult
Males
Mean
10001
9397
8822
8844
8548
8037
7788
7228
7181
8187
9043
10119
11913
.0
.0
.2
.4
.3
.0
.4
.2
.1
.1
.4
.0
.7
S.D.
1211
809
582
799
681
774
855
648
766
562
1202
780
1613

.6
.6
.9
.9
.6
.1
.6
.2
.3
.4
.2
.5
.9
Adult Females
N
13
23
22
15
22
15
20
9
5
9
7
-_
Mean
7800
7639
7145
6671
6235
6317
5778
5946
6680
7201
7634
—
.0
.9
.9
.3
.2
.4
.0
.0
.8
.4
.7

S.D.
795.8
1116.4
785.2
752.3
538.1
693.9
753.5
1192.7
1708.8
1254.8
864.7
—
Juvenile
N
--
--
2
5
6
21
19
32
38
28
11
Mean
--
--
6336.
4366.
4815.
4903.
5259.
6044.
7858.
8866.
9955.
Males



2
9
7
4
8
8
5
6
1
S.D
--
--
--
741
450
369
715
1552
1456
1530
841




.6
.6
.9
.7
.8
.8
.8
.8
Juvenile
N
--
--
--
1
1
14
12
20
30
19
4
Females
Mean
--
--
--
4461
3591
4117
4624
4909
6611
7455
7964



.6
.5
.3
.8
.6
.8
.0
.7
S.D
--
—
--
--
--
562
1082
751
1665
1228
717






.9
.6
.4
.2
.7
.8

-------
feeding  results  in  decreased  gizzard size and  increased  feeding,  as in pre-
migratory  hyperphagia,  results  in  hypertrophy  (Breitenbach  et al.,  1963;
Anderson, 1972; Moss,  1974; Ankney, 1977).

     Gizzard  weight decreased  significantly  from April to  May in adult male
meadowlarks  (P <  0.05).  It then increased substantially  during the last two
months  of  the season  (P < 0.01).  Contents of  the  gizzards of our  specimens
were also weighed and  categorized at  3-hr intervals  throughout the day.
No diurnal feeding  pattern was  apparent.   Uncertainties regarding rate of food
passage in the gut make these data difficult to  evaluate.


Molt

     Postnuptial  molt  in  the  population  lasted from  July through the  end of
collecting and tended  to begin  earlier in  males  than in females  (Table 22.25).
A complete molt involving  flight  feathers  occurred also in juveniles  and their
molt  had  approximately  the   same  tempo  as  that  of adults   (Table 22.25).
Weights  of the dry  integument  increased  toward  the  end of  the  season as new,
unworn feathers replaced the old (Table 22.26).

     Molt and reproduction in most temperate  zone migrants  do not overlap in
time, a  relationship that  seems  to hold  for  all species  in the present study
(Lewis, Morton and Kern; unpublished data).

     Lean body mass  was  relatively stable during molt  in our meadowlarks,  a
phenomenon also  observed  in  chaffinches   (Fx>i,ngi>11a ooelebs )  by Gavrilov and
Dolnik  (1974),  in   European tree sparrows  (Passer1 m.. montanus ) by Myrcha and
Pinowski  (1970) ,  and white-crowned  sparrows ( ZonotT-iah-ia leucophpys gambel-i-i^
by  Chilgren  (1977).   Such  stability suggests  that  feather  growth was  not
achieved at the expense of  body protein.

     We  analyzed  data  on  body  lipid  as   a function  of molt  stage to better
appreciate  the  relationship  of molt  to onset  of  premigratory — fattening.
Results  show that  as  the  molt comes to  a close,  meadowlarks  begin to fatten
(Table 22.27).  Birds  having completed or  nearly completed molt  (category 0-1)
had  significantly more body lipid than those  still  growing two or more pairs
of  remiges   (P  <  0.01).   Thus  molt within  the  population  was not  perfectly
synchronous.

     Slight  increases  in body weight during postnuptial  molt have been docu-
mented  for a number of migratory species, usually this was attributed to the
new  plumage.   In at least one case,  however, a major increase in weight was
due to fattening (Morton and Welton,  1973).
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Adolph,  E.  F.  and F.  W.  Hegeness.  1971.   Age  Changes  in Body Water  and  Fat  in
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                                      307

-------
     TABLE 22.27.  BODY L1PID AS PERCENT OF BODY WEIGHT IN WESTERN MEADOWLARKS DURING AND AT END OF MOLT
u>
o
oo

Adult Males

N
Mean
S.D.
6+
6
3.91
0.92
2-5
10
5.65
0.94
0-1
5
9.92
3.08
Adult Females
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4.13
0.75
2-5 0-1
9 2
6.33 8.51
1.65
Juvenile Males
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36
4.31
0.96
2-5
13
5.73
2.61
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8
9.49
3.49
Juvenile Females
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22
4.65
1.58
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13
5.18
0.87
0-1
3
12.69
0.50
All Birds
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75
4.36
1.15
2-5
45
5.67
1.72
0-1
18
10.03
3.10

     *  Category 6+ means  six  or more  pairs  of  remiges  still  had  to grow in,  2-5 means two to five pairs .miges

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       been completed.

-------
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                                     314

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                     SECTION 23

  PARTICULATES IN THE LUNGS OF WESTERN MEADOWLARKS
     (STURNELLA NEGLECTA) IN SOUTHEASTERN MONTANA

      M. D. Kern, R. A. Lewis and M. B. Berlin
                      ABSTRACT

     The lungs of western meadowlarks (Sturnella
negleota), collected within 100 km of the coal-fired
power plant and coal mines at Colstrip, Montana, were
examined histologically for particulates and associated
pulmonary damage.  Birds were collected during 1975
(when the power plant was not operating), 1976 (when it
operated intermittently), and 1977-78 (when it was in
full operation).

     Three major categories of particulates occurred in
the meadowlark's lung: (1) crystals of variable size,
(2) very small ("50.5 ym) round black flecks, and
(3) larger black particles of variable size and shape.
Most larger particles were confined to the air ducts,
but smaller ones were widespread in the lungs.  Crystals
were the only particulates that irritated pulmonary
tissue, sometimes eliciting mild fibrosis within the
parabronchial wall.

     Particulates, especially the black forms,
increased in the lining of the parabronchi and the
lumen of the air capillaries between 1975 and 1977.
The number of particulate-containing macrophages in
the lining of the parabronchi also increased between
1975 and 1976, but then declined.  However, in 1978,
the particulate content of the lung was at 1975 levels
and there were fewer particulate-containing macrophages
in the parabronchi than in 1975.  These declines are
probably related to the fact that most of the meadow-
larks collected in 1978 were obtained at greater
distances from Colstrip than birds collected in 1976-77.

     Juvenile birds had smaller particulate burdens
than adults.   Among juveniles collected in 1977 and
                         315

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             1978, the concentrations of participates were
             similar in the parabronchi, but significantly
             different in the air capillaries (smaller in
             1978).   Particulate burdens of male and female
             birds were similar in all but one region of the
             lung.  The number of particulate-containing
             macrophages was negatively correlated with the
             distance from Colstrip at which a bird was
             collected during 1975-77.
                                INTRODUCTION

     Birds have the potential to serve as biological monitors of
particulate air pollution from coal-fired power plants.  Small birds have
high metabolic rates and are active at levels where exposure to gaseous and
other respirable pollutants may be severe (Lewis and Lewis, 1979).  Their
lungs are a major site of detoxification and contain macrophages that remove
particulate matter from inhaled air.  Their pulmonary tissue is easily
irritated by inhaled substances to which it exhibits inflammatory responses
of greater or lesser severity.  In this respect, birds appear to be an order
of magnitude more sensitive to aerial pollutants than are humans (Takemoto
et al., 1974).  Since little respired material is filtered out in the nasal
passageways (Takemoto et at., 1974) and air flow through the lung is only in
one direction (Bretz and Schmidt-Nielsen, 1971), the avian lung is analogous
to a high volume sampler of air-borne materials.

     The few published reports concerning the effects of air pollutants on
wild birds generally pertain to sedentary urban species and support their use
as biomonitors (Lewis and Lewis, 1979).  The most striking case of historic
importance is the use of the canary (Serinus eanari-d) in sensing mine gases
and anoxia (Neal and Olstruin, 1971).  Levels of lead in the organs of pigeons
(Columbia livid}, both in Japan and the United States, have been related to
aerosol levels of this element at sampling sites (Tansy and Roth, 1970; Ohi
et al. , 1974).  Similar relationships have been discovered between the dust
content and associated damage in the lungs of doves and pollutant levels at
sampling sites in Japan (Takemoto et al., 1974); and between the presence of
particulate-laden pulmonary macrophages in the lungs of house sparrows
(Passer domesticus)  and pollution levels in areas of California (McArn et al.,
1974).   In addition, Tashiro et al. (1974) have demonstrated that birds are
especially sensitive to air-borne pollutants during their breeding season.
Takemoto et al.  (1974) found a direct relationship between the age of doves
in polluted regions  of Japan and the degree of lung damage.

     Western meadowlarks (Sturnella negleota) are the most widely distributed
and abundant passerine in the Colstrip area (Lewis et al., 1976; Preston and
Thompson, 1979).   They are neither sedentary nor urban, but presumably return
to nest in the same  general vicinity year after year (Lewis, unpublished
banding returns).  Consequently, individuals may be exposed to aerial
emissions from the Colstrip power plant for five months each year at a time
when they are reproductively active and hence potentially highly sensitive

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 to such insults on the respiratory system.   Furthermore, unless  they  can
 completely clear particulates from their lungs while absent  from Montana
 (which does not seem to be the case),  there may be accumulation  of
 particulates in the respiratory system with successive years of  exposure.
 Under  these conditions, western meadowlarks may be particularly  useful
 biomonitors of  stack emissions in remote grassland areas surh as Colstrip.

                            MATERIALS AND METHODS

     This  study deals with samples of  lungs from western meadowlarks
 (S.  neglecta} collected within 100 km  of Colstrip,  Montana,  between 1975 and
 1978.   Most birds were taken SSE and SEE of Colstrip,  i.e.,  from sites that
 are predominantly downwind of the power source (Miller et al., 1976;  Crecelius
 et al.,  1978).   Birds were shot and dissected  in the field as described by
 Lewis  et al.  (1976).   The  caudal tip of the left lung  was removed from each
 bird and fixed  in Bouin's  solution or  10 percent neutral buffered formalin.
 Fixed  samples were later dehydrated, embedded  in paraffin, and sectioned at
 7.0 urn.  Representative sections were  stained  with haematoxylin  and eosin by
 American Histolabs (Silver Spring,  Md.)  and examined by us.

     Our histological survey of the lung is modeled after methods of McArn
 et at.  (1974).   Initially,  we scanned  the sections  in  order  to determine the
 types  of particulates that were present.  Then,  we  examined  20 transverse
 sections of  parabronchi and five regions of air  capillaries  selected  at
 random within each section more closely.  "We determined the  particulate
 concentrations  in (1)  macrophages and  smooth muscle cells within the  lining
 of  each parabronchus,  (2)  the lumen of  each parabronchus, and  (3) the lining
 and  lumen  of the  air  capillaries,  in each case using a scale of  0 (none
 present) to  5 (very high concentrations  present).   In  addition,  we counted
 the  number  of particulate-containing macrophages in the lining of each of
 the  20  parabronchi.

                            RESULTS  AND DISCUSSION

Histological Structure of  the Meadowlark's  Lung

     We  begin with a  brief  statement concerning  the microscopic  anatomy of
 the meadowlark's  lung  because  it  has not  been  described previously.   The
meadowlark's lung  is  structurally  similar to that of the domestic fowl
 (Hodges, 1974).   However, pulmonary lobules, consisting of a parabronchus and
the air  capillaries that arise  from it,  are  not as  clearly defined as in
chickens.  There  is no conspicuous  connective  tissue partition between
adjacent lobules.  In  the  terminology of Hodges  (1974), atria, infundibulae,
and air  capillaries are all represented  in  the lobule.

Nature of the Particulates  in the Meadowlark's Lung

     The lungs of our  specimens contained three basic  types of particulates
(Figure  23.1):

     1.  Transparent,  tetragonal crystals, ca.  1.5 urn  in length and  0.5 ym
         in width, scattered individually or in clusters and chains.


                                     317

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                                                           /

Figure 23.1.
Particulates (arrows) in the lungs of western
meadowlarks collected near Colstrip, Montana.

A and B.  Crystalline particulates of small and
large size.  C.  Spherical black particles within
macrophages on the border of a parabronchus.
D.  Large black particulates with distinct
projections in an area of air capillaries.
Magnification:  A - C, 3750X; D, 7500X.
                               318

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     2.  Small round black flecks with a diameter ^0.5 ym.

     3.  Larger black particles; these were round, oval, triangular,
         polygonal, splinterlike, or irregular in shape and varied in
         size with minimal dimensions between 0.9 and 12.0 ym and maximal
         dimensions between 1.4 and 21.6 ym.  They were sometimes con-
         glomerates of the small flecks.

Black filamentous material and large irregular crystals were also
occasionally present.  The latter commonly measured between 2.8 and 32.9 ym
on a side.  Most of the larger particulates were confined to the air ducts,
whereas smaller particulates were widespread in both the air ducts and air
capillaries.

     The parabronchial wall was occasionally thickened around small groups of
crystalline particulates.  This suggests, as does their size, that they are
silicates since (1) the latter are known to elicit fibrotic responses from
pulmonary tissue (Bowden, 1976), and (2) one of the major particulates in
aerosols near Colstip is an aluminum silicate of a size (0.6 to 1.0 ym)
similar to the crystals in the meadowlark lung (Van Valin et al., 1979).

     On the basis of their spherical shape and tiny size, the small flecks
in the meadowlark's lung may be sulfur- or chlorine-containing particulates
emitted by the power plant (Van Valin et al., 1979).  These particles and the
larger black ones rarely elicited inflammatory responses from the birds'
pulmonary tissue aside from occasional small infiltrations of lymphocytes
around major blood vessels.  Extravasation frequently occurred around heavy
concentrations of black particulates, but may be an artifact of the dissection
procedure because (1) other heavy concentrations of particulates in the same
sections were not enveloped by erythrocytes, and (2) parabronchi were commonly
filled with erythrocytes.

Particulate Burdens of the Meadowlark's Lung

     The distribution and density of particulates in the meadowlark's lung
appear in Table 23.1.  To our knowledge, this is the first time that changes
in particulate burdens have been examined for several months of each of
several years, and with regard to age and sex, in an avian species.

     Particulate burdens in the meadowlark's lung increased progressively
between 1975 (when the power plant was not operating), 1976 (when it operated
intermittently), and 1977 (when it was in full operation).  This trend is
especially well shown by the particulate content of macrophages in the lining
of the parabronchi.   However, it is also reflected by changes in particulate
density at other sites in the parabronchus, and in the lumen of the air
capillaries, although not in the lining of the latter.

     All types of particulates increased, but the change in the black forms
was especially noticeable (Figure 23.2).  Lungs of many adult birds collected
in 1975 were completely free of particulates.  This was not the case in
subsequent years.   The change in particulate burdens was especially
                                     319

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TABLE 23.1.  PARTICULATE  CONTENT OF LUNG TISSUE FROM WESTERN MEADOWLARKS  (5 turnella neglecta)
             COLLECTED  AT COLSTRIP, MONTANA, BETWEEN 1975 AND 1978*1"
Particulates associated with parabronchi
Number of
Groups N containing
macrophages per Macrophages
parabronchus (rated 0-5)
Adults:
1975 29 24. 81 ±3. 99 a 1.38 ±0.21
1976 41 30.43±4.26 b 2.19±0.24
U> 1977 130-131 22.64 + 1.06 a 2. 45 ±0.18
NJ
O
1978 27 18.29 + 1.31 c 1.67±0.26
Juveniles:
1977 15 31.05±5.40 a 1.91±0.38
1978 15 27. 43 ±2. 74 a 1.46 + 0.43
Adults:
April 1976-1977 43 27.20±3.76 a 2.07±0.27
May 1975-1977 65 24. 27 ±2. 21 ab 2. 11 ±0.23


Particulate density in
Particulates associated with
air capillaries


Smooth muscle Lumen of Lining of air Lumen of air
cells parabronchus capillaries capillaries
(rated 0-5) (rated 0-5) (rated 0-5) (rated 0-5)

a 1.15 + 0.18 a 0.88 + 0
b 1.31 ± 0.13 a 0.73 ± 0
b 1.60± 0.12 b 1.16 ± 0

a 1.08 + 0.16 a 0.90+0

a 1.34 ± 0.29 a 0.98 ± 0
a 0.98 ± 0.35 a 0.89 ± 0

a 1.26 + 0.19 a 0.88±0
a 1.39±0.14 a 1.09±0
[1975,
0.62 + 0
[1976]

.16 a 1.93 + 0.27
.11 a 1.90±0.18
.09 b 1.95±0.09

.12 a 1.64 ±0.11

.23 a 1.73±0.32
.26 a 0.88 ± 0.36

.14 ab 1.90 ±0.21
.15(49) be 1.88 + 0.13
1977]
.ll(16)a


a 0.40+0.11 a
a 0.40 ± 0.10 a
a 0.63 ±0.07 b

a 0.47 + 0.11 ab

a 0.44 ±0.09 a
b 0.24 + 0.09 b

a 0.60 ± 0.12 ab
a 0.47 + 0.10 a


                                                                       (continued)

-------
             TABLE  23.1.    (Continued)
Co
Particulates associated with parabronchi
Number of
Groups N containing
macrophages per Macrophages
parabronchus (rated 0-5)
Particulate density in
Particulates associated with
air capillaries

Smooth muscle Lumen of Lining of air Lumen of air
cells parabronchus capillaries capillaries
(rated 0-5) (rated 0-5) (rated 0-5) (rated 0-5)
June 1975-1977 68 21 . 87 ± 1 . 51(63) b 1.28 + 0.321 9) a 1 . 1 5 ± 0. 16(14) a ]. 22 ±0.12
[1975,1977] [1975] [1975,1976]
33.48±1800( 5)a 2. 51 ± 0. 22(59) b 1 .88 ± 0.14(54) b
[1976] [1976,1977] [l97?]

July 1975, 28 22. 64 ±2. 49 ab 1. 89±0.45
1977-1978

August 1975,1978 22 20. 77 ±3. 61 b 1.57*0.30
Males 171 24.72±1.36 a 2. 19 t 0.18
Females 89 24. 53 ±2. 19 a 1. 94 ± 0.18
Adults 227 23. 61 ±1.19 a 2. 17 ±0.13
Juveniles 33 31. 85 ±3. 20 a 1.67 ±0.27

a 0.85 ± 0.24(13)a 0.97 + 0.20
[1975,1978]
1.79± 0.47(15)ab
[1977]
a 1 .07 ± 0.20 a 0.87 i 0.13
a 1.43 ± 0.10 a 1 .06 ± 0.08
a 1.31 ± 0.12 a 0.90 ± 0.10
a 1.43 ± 0.08 a 1.02 ± 0.07
b 1.13 ± 0.21 b 0.93 ± 0.15
c 2.33±0.37( 9) a 0. 36 i 0. 18(14) a
[1975] [1975,1976]
1.76±0.69( 5)a 0. 65 ± 0. 09(54) b
[1976J [1977]
1.96± 0.10(54)a
[1977]
abc 1.93 ±0.27 a 0.51 ±0.16 ab

abc 1.68 ±0.14 a 0.46+0.12 ab
a ].86±0.09 a 0.43 ±0.08 a
b L,76±0.13 a 0.45 + 0.07 a
a 1.90 ±0.07 a 0.54 ±0.05 a
a 1.30+0.26 b 0.34±0.07 b
              *Values  In  the  table are means t C195(N).  For the monthly  changes  in  the particulate content of the adult  lung,  statistically
               significant differences existed between years of the study;  data were  lumped whenever possible, but in some  cases  were neces-
               sarily  present.ed  separately.
              "Within  t.he  column  in each division of the table, values  not.  followed by  the same letter differ significantly  at  the 0.05 level
               (Student,  t-tests and Student-Neuman-Keuls tests for data concerning the number of macrophages; Mann-Whitney or Student-Neuman-
               Keuls  tests for rated data).

-------
                               •
                                •
                         •*.' »•;
                        •••*••<-•
                         »_j-*
    r
  'f • -
         . -"v'*1^,
             -
  . .;
  ''.'•
Figure 23.2.  Changes in the particulate content of lungs  from
              western meadowlarks collected between 1975 and  1977.

              A and B.  During 1975, the lining of the  parabronchus
              (P) and air capillaries (C) was frequently free of
              particulates.  C and D.  During 1977, particulates
              occurred in the lining of both parabronchi and  air
              capillaries (arrows).  Magnifications:  A and C,  750X;
              B and D, 3750X.
                                 3Z2

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pronounced in macrophages within the lining of the parabronchi.  Curiously,
the number of these macrophages declined in 1977, although the actual
particulate content of the parabronchi increased.

     In 1978, the particulate content of the lung was similar to that seen
in 1975.  Furthermore, significantly fewer particulate-containing macrophages
occurred in the parabronchi than in 1975.  There are several possible
explanations for these declines.  Most important in this regard is the fact
that birds shot in 1978 were intentionally collected at distances in excess
of 69 km from the power plant in order to supplement the pre-operational data
base for the Colstrip Project.  Collections in earlier years were frequently
made much closer to the power plant.  However, since birds with dirty lungs
were collected at these great distances in earlier years, other factors may
also be responsible for the decreases in 1978.  Perhaps meadowlarks are now
actively avoiding heavily impacted areas near the power plant, as suggested
by the data of Preston and Thompson (1979), and therefore are exposed to fewer
air-borne aerosols than in earlier years.  However, we cannot discount the
possibility that mechanisms for removing particulates from the lungs have
improved (i,.e.} adapted to the increased particulate burdens) during the 4
years of study.  Bowden (1976) has shown, for example, that the number of
alveolar macrophages in the mammalian lung is directly related to the number
of small particles that reach the alveoli (also see Stuart, 1976).  It is also
possible that the age structure of the adult segment of the population in
1978 was weighted toward young adults.  This may be significant in light of
the finding of Takemoto et a.1. (1974) that the trauma produced by aerosols
in avian lungs is directly related to the age of birds.  We suspect, however,
that the declines in 1978 are due largely to the collection procedures
followed  that year.

     Significant differences in the particulate burdens of adult lungs
existed between the months when the birds were collected.  However, we are
unable to discern general trends in the data because of differences in some
months (e.g. June) over the 4 years of study and because monthly changes
in one region of the lung are not in the same direction as changes elsewhere
in the same lung (Table 23.1).  If a small sample of five birds collected in
June, 1976, is ignored, it is possible to conclude that the number of
particulate-containing macrophages in the parabronchi was higher during
April than between May and August.

     Significant differences in particulate burdens as a function of age
were observed;  juvenile birds had cleaner lungs (Table 23.1).  Among the
juveniles collected during 1977 and 1978, the concentrations of particulates
in the parabronchi were similar, but concentrations in the air capillaries
differed significantly (lower in 1978) .  The particulate burdens of male and
female meadowlarks were similar in all but one region of the lung that were
examined.

Pollution Gradient Analysis

     Our study appears to be the first to provide a pollution gradient
analysis based on the avian respiratory system.   The number of particulate-
containing macrophages per parabronchus declined as the distance between the


                                     323

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site of collection and the power plant increased during 1975, 1976, and 1977,
but not during 1978 (Table 23.2).  Given the great minimal distance from
Colstrip (and the smaller dispersion about the mean) at which meadowlarks
were shot during 1978 (69 km), the absence of a relationship during that year
is probably not surprising.  The inverse relationship between the two
variables in each of the earlier years is both linear and significant,
although weak (Table 23.2).

     Whereas significant relationships existed between the mmbev of
particulate-containing macrophages and collection distance during 1975-77,
only one significant relationship occurred between par't'Lculate density in the
parabronchus or air capillaries and collection distance (Table 23.3).  These
findings, and the large amount of particulate matter accumulated by pulmonary
macrophages (Figure 23.2), suggest that the number of particulate-laden
macrophages is the most sensitive indicator of pollution impact on the birds.
Data concerning the number of such cells are relatively easy to obtain and
may be a sensitive bioindicator of the power plant's impact on birds until
and unless the air ducts become saturated with particulates because of
repeated exposure to aerosols.  Clearly, further information on power plant
emissions and air quality in the vicinity of Colstrip is needed and birds
may prove useful in its acquisition.

     In this regard, it is worth adding that our data are consonant with
data obtained with air quality monitoring equipment at Colstrip (Crecelius
et at., 1978).  Using the latter, it  has been demonstrated that 69 percent (by
weight) of the stack dust at Colstrip is less than 0.3 ym in diameter and
hence can remain air-borne for days or weeks and be widely dispersed.  A
continuously recording air quality monitoring station situated 12 km
downwind (SE)  from Colstrip has also  recorded plume strikes several times
each week when the power plant was in operation.

     It is possible, but remains to be demonstrated, that the avian lung is
a more sensitive and reliable sampler of low levels of air-borne particulates
than state-of-the-art monitoring equipment.  In contrast to the data from
meadowlark lungs (Table 23.1), the equipment did not record significant
changes in the concentration of elements in Colstrip air after Unit 1 of the
power plant began operating.

Recommendations

     Since the particulates in the lungs of western meadowlarks at Colstrip
may originate from several sources (fugitive dust from traffic on secondary
roads or that associated with farming and mining operations; stack emissions
of the power plant), it is important  to distinguish the impact of the power
plant from other potential impacts.  Consequently,  we recommend that samples
of lung be set aside in the future (1)  for trace metal analysis, and (2) for
examination with the electron microscope, as well as for histological
examination.

     Atomic absorption analyses of trace metals should indicate if emissions
from the power plant are accumulating in the birds' lungs.   The stack dust at
Colstrip is relatively rich in Ca, Se and V.   Concentrations of these elements

                                     324

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        TABLE 23.2.  DENSITY GRADIENT ANALYSIS:  NUMBER OF PARTICULATE-CONTAINING MACROPHAGES
                     PER PARABRONCHUS VS. DISTANCE  OF MEADOWLARK  FROM  COLSTRIP AT CAPTURE
OJ
         Year    N
Mean distance from
Colstrip at capture
 [km(range)]
Linear relationship
between number of
macrophages (Y) and
distance from
Colstrip in km (X)*
Correlation
coefficient
for the
equation (r)
Significance
     of
correlation
coefficient
1975
1976
1977
1978
22
44
146
42
74.7
60.3
62.4
74.3
(38.94 -
(20.92 -
(18.10 -
(68.80 -
90.12)
96.56)
96.96)
89.31)
Y =
Y =
Y =
Y =
57.30 -
48.16 -
27.92 -
17.12 +
0.40
0.27
0.07
0.06
X
X
X
X
-0
-0
-0
+0
.48
.39
.25
.07
0.02 0.50

         *The slopes (regression coefficients)  of  these four  equations  are not  statistically
          different (P>0.05;  analysis of covariance)

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TABLE 23.3.  THE RELATIONSHIP BETWEEN PARTICULATES IN THE
             LINING OF THE PARABRONCHI AND AIR CAPILLARIES
             VS. DISTANCE OF THE MEADOWLARK FROM COLSTRIP
             AT CAPTURE, AS SHOWN BY THE CORRELATION
             COEFFICIENTS, IS NOT USUALLY LINEAR

Correlation coefficients (r)
Year N
1975 22
1976 44
1977 146
1978 42
Lining of
parabronchus
-0.11
-0.23
+0.21*
+0.18
Lining of air
capillaries
+0.15
+0.08
-0.04
+0.07
"0.01 
-------
(and several others) have been measured in dust at three air monitoring sites
near Colstrip (Crecelius et al., 1978).  Assays of these elements in samples
of lung may more closely establish the contribution of the power plant to the
observed particulate burdens in the tissue.

     However, atomic absorption analyses will not indicate the distribution
of these and other particulates in the lungs nor the damage they cause to
pulmonary tissue.  Hence, routine histological surveys should be continued.
They should be complemented with ultrastructural studies, similar to those
done by McArn et al. (1974), in order to clearly identify particulates of
very small size in the lung.

     One limitation of the study to-date involves the method used to fix the
lungs.  Extravasation is commonly widespread in the organ and fixation is not
uniformly good.  These shortcomings confound histological evaluation and can
be readily avoided if in the future the air duct system of the bird is
perfused with fixative before the lung is removed and fixed.  This method of
fixation will also preserve the larger ducts in the respiratory tree.  It
would be useful to study the effects of particulates on the mucociliary
apparatus of these larger airways since they are known to be affected by
exposure to such things as SC>2 in other species of birds (Wakabayashi et al,,,
1977) .  In addition, a considerable fund of information concerning the
structure of these larger airways of birds, both at the light and electron
microscopic levels, is already available in the literature and therefore
readily available for comparison (Bienenstock et al., 1973; Hodges, 1974;
Walsh and McLelland, 1974 a,b; Jeffery, 1978).

                                CONCLUSIONS

     The meadowlark's lung is structurally similar to that of the domestic
fowl.

     Three major categories of particulates occurred in the meadowlark's lung
during 1975-78:   (a) crystals of variable size, (b) small C< 0.5 urn) round
black flecks,  and (c) larger black particles of variable size and shape.  The
crystals may be silicates.   The small flecks may be sulfur- or chlorine- con-
taining particles emitted by the power plant.   Larger particles were generally
confined to the air ducts,  but smaller ones were widespread in the lungs.
Only the crystals caused perceptible irritation to the lung.

     All categories of particulates, but especially the black forms, increased
in the lining of the parabronchi and the lumen of the air capillaries between
1975 and 1977.  The number of particulate-containing macrophages in the lining
of the parabronchi also increased between 1975 and 1976, but then declined.
In 1978, the particulate content of the lung was at 1975 levels and there were
fewer particulate-containing macrophages in the parabronchi than in 1975.
These declines are probably related to the fact that most of the meadowlarks
collected in 1978 were obtained at greater distances from Colstrip than birds
collected in 1976-77.

     Significant monthly variations in particulate burdens occurred at  the
various sites of the lung that were examined,  but overall monthly trends are


                                     327

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difficult to discern.   However,  the number of particulate-containing macro-
phages was,  with one exception,  higher during April than between May and
August.

     Juvenile birds had smaller  particulate burdens than adults.

     Among the juveniles collected in 1977 and 1978,  the concentrations of
particulates were similar in the parabronchi, but significantly different in
the air capillaries (smaller in  1978).

     Particulate burdens of male and female birds were similar in all but one
region of the lung that were examined.

     The number of particulate-containing macrophages was significantly and
negatively correlated with the distance from Colstrip at which a bird was col-
lected during 1975, 1976, and 1977-

     Only one significant relationship (weak and positive) occurred between
particulate density in the lung  and the distance from Colstrip at which a
meadowlark was collected.

     Of the histological measurements, the number of  particulate-laden macro-
phages in the lining of the parabronchi appears to be the most sensitive in-
dicator of pollution impact on meadowlarks.   It appears to be a useful bio-
monitor of the particulate output of the coal-fired power plant at Colstrip.
                                 REFERENCES

Bienenstock, J.,  N.  Johnston,  and D.Y.E.  Perey.   1973.   Bronchial Lymphoid
    Tissue.  I.   Morphologic Characteristics.  Lab.  Invest.,  28(6):686-692.

Bowden, D.H.  1976.   The Pulmonary Macrophage.   Env.  Health Persp.,  16:55-60.

Bretz, "W.L., and  K.  Schmidt-Nielsen.   1971.  Bird Respiration:  Flow Patterns
    in the Duck Lung.   J. Exp.  Biol.,  54:103-118.

Crecelius, E.A.,  L.A.  Rancitelli, and  S.  Garcia.   1978.   Power  Plant Emissions
    and Air Quality.   In:  Potential  for  Gaseous and Heavy Metal Contamination
    from Energy Extraction Processes  in the Northern Great Plains, DOE Annual
    Report, September, 1978, (unpublished), J.J.  O'Toole and  C.C. Gordon,
    eds. pp. 9-33.

Hodges, R.D. 1974.   The Histology of  the  Fowl.   Academic Press, Inc., New
    York.  648 pp.

Jeffery, P.K.   1978.   Structure and Function of  Mucous-Secreting Cells of Cat
    and Goose Airway Epithelium.   Ciba Foundation Symp., 57:5-23.
                                      328

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Lewis, R.A., and C.W. Lewis.  1979.  Terrestrial Vertebrate Animals  as
    Biological Monitors of Pollution.  In:  Monitoring Environmental
    Materials and Specimen Banking, N.-P. Luepke, ed.   Martinus  Nijhoff
    Publ., The Hague,  pp. 369-391.

Lewis, R.A., M.L. Morton, and S.C. Jones.  1976.  The  Effects of Coal-Fired
    Power Plant Emissions on Vertebrate Animals in Southeastern  Montana
    (A Report of Progress).  In:  The Bioenvironmental Impact of A Coal-Fired
    Power Plant, Second Interim Report, Colstrip, Montana,  June, 1975,
    R.A. Lewis, N.R. Glass, and A.S. Lefohn, eds.  EPA-600/3-76-013,  U.S.
    Environmental Protection Agency, Corvallis, Oregon,  pp.  140-187.

McArn, G.E., M.L. Boardman, R. Munn, and S.R. Veilings.  1974.  Relationship
    of Pulmonary Particulates in English Sparrows to Gross  Air Pollution.
    J. Wildlife Dis., 10:335-340.

Miller, J.R., T.Cail, and A.S. Lefohn.  1976.  Air Monitoring
    Characterization at the Hay Coulee Site, Colstrip, Montana.   In:  The
    Bioenvironmental Impact of A Coal-Fired Power Plant,  Second  Interim
    Report, Colstrip, Montana .  R. A. Lewis, N. R. Glass,  and
    A.S. Lefohn, eds.  EPA-600/3-76-013, U.S. Environmental Protection
    Agency-, Corvallis, Oregon.  pp. 213-221.

Neal, J.E., and E.G. Olstrum.  1971.  Birdlife - An Indicator of Environmental
    Quality.  Ext. Bull. E-707, Natural Resources Series, Cooperative
    Extension Service, Michigan State Univ., East Lansing,  Mich. 4 pp.

Ohi, G., H. Seki, K. Akiyama, and H. Yagyu.  1974.  The Pigeon,  A Sensor of
    Lead Pollution.  Bull. Env. Contamination Tox., 12(1):92-98.

Preston, E.M., and S.K. Thompson.  1979.  Trends in Bird Populations in  the
    Vicinity of Colstrip.  In:  The Bioenvironmental Impact of A Coal-Fired
    Power Plant, Fourth Interim Report, Colstrip, Montana.
    E.M. Preston and T.L. Gullett, eds.  EPA-600/3-79-044,  U.S.
    Environmental Protection Agency, Corvallis, Oregon.  pp.  240-256.

Stuart, B.O.  1976.  Deposition and Clearance of Inhaled Particles.   Env.
    Health Persp., 16:41-53.

Takemoto, K., H. Katayama, K. Namie, R. Endo, and K. Tashiro. 1974.  Effects
    of Air Pollution on the Ornitho-Respiratory System.  Part IV. Pathology
    of Doves Lung.  Jap. J. Hyg., 29(1):106.

Tansy, M.F., and R.P- Roth.  1970.  Pigeons: A New Role in  Air Pollution.
    J. Air Poll. Cont. Ass., 20(5):307-309.

Tashiro, K., K. Namie, K. Takemoto, and E. Hisazumi.  1974.  Effects of  Air
    Pollution on the Respiratory System of Animals in  a Zoological Garden.
    Jap. J. Hyg., 29(1):107.
                                     329

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Van Valin, C.C., R.F. Pueschel, D.L. Wellman, N.L.  Abshire,  G.M.  Lerfald,  and
    G.T. McNice.  1979.  Aerosol Characterization in the Vicinity of
    Colstrip, Montana.  In:  The Bioenvironmental Impact of  A Coal-Fired
    Power Plant, Fourth Interim Report,  Colstrip, Montana.
    E.M. Preston and T.L. Gullett, eds.   EPA-600/3-79-044, U.S.
    Environmental Protection Agency, Corvallis,  Oregon,   pp. 2-52.

Wakabayashi, M., B.C. Bang, and F.B. Bang.   1977.  Mucociliary Transport in
    Chickens Infected with Newcastle Disease Virus  and Exposed to Sulfur
    Dioxide.  Arch. Env. Health, 32(3):101-108.

Walsh, C., and J. McLelland.  1974a.  The Ultrastructure of  the Avian
    Extrapulmonary Respiratory Epithelium.   Acta Anat.,  89:412-422.

Walsh, C., and J. McLelland.  1974b.  Granular "Endocrine" Cells  in  Avian
    Respiratory Epithelia.   Cell Tissue  Res., 153(2):269-276.
                                     330

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                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing/
1. REPORT NO.
4. TITLE AND SUBTITLE
                              2.
                                                           5. REPORT DATE
The  Bioenvironmental  Impact  of a Coal-Fired Power Plant;
Sixth  Interim Report,  Colstrip,  Montana.  August, 1980."
             6. PERFORMING ORGANIZATION CODE
                                                           3. RECIPIENT'S ACCESSION NO.
1. AUTHOR(S)   "                        ~~~	
Edited by  Eric M. Preston,  David W. O'Guinn, and
           Ruth A. Wilson
             8. PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AND ADDRESS
 U.  S.  EPA
 Corvallis Environmental  Research Laboratory
 200 S.W.  35th St.
 Corvallis, OR  97330
             10. PROGRAM ELEMENT NO.
             11. CONTRACT/GRANT NO.
12. SPONSORING AGENCY NAME AND ADDRESS

 SAME
             13. TYPE OF REPORT AND PERIOD COVERED
              Interim  12/77—12/80	
                                                            14. SPONSORING AGENCY CODE

                                                             EPA/600/02
15. SUPPLEMENTARY NOTES  In  this  series the EPA numbers  are:  the 1st Interim Rept.  (EPA-
 600/3-76-002), the 2nd  Interim Rept. (EPA-600/3-76-013),  the 3rd Interim Rept.  (EPA-
 600/3-78-021), the 4th  Interim Rept. (EPA-6QO/3-79-Q44),  and the 5th Interim Rept.  (EPA-
16. ABSTRACT                                                         --       600/3~80-052).
      The EPA has recognized the need for a rational  approach to the incorporation  of
 ecological impact information into power facility  siting decisions in the northern
 great plains.  Research  funded by the Colstrip,  Coal-Fired Power Plant project  is  a
 first attempt to generate methods to predict  the bioenvironmental effects of air
 pollution before damage  is sustained.  Pre-construction documentation of the environ-
 mental characteristics of the grassland ecosystem  in the vicinity of Colstrip,  Montana
 began in the summer  of 1974.   Since then, key characteristics of the ecosystem  have
 been monitored regularly to detect possible pollution impacts upon plant and animal
 community structure.
      In the summer of 1975, field stressing experiments were begun to provide the  data
 necessary to develop dose-response models for S02  stress on a grassland ecosystem.
 These experiments involve continuous stressing of  one acre grassland plots with _
 measured doses of S02 during  the growing season (usually April through October).
      Results of the  1979 field season's investigations are summarized in this
 publication.  This is the last interim report of the six year project.  Final reports
 will be published in 1981.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.IDENTIFIERS/OPEN ENDED TERMS
                           c. COSATI Field/Group
 plant and animal response to pollution
 coal-fired power plant
 air pollutants
 grassland ecosystems
 coal-fired power  plant
               emissions
 air quality monitoring
       51
18. DISTRIBUTION STATEMENT

 release to public
19. SECURITY CLASS (This Report)
 Unclassified	
21. NO. OF PAGES
 330
                                              20. SECURITY CLASS (This page)

                                                Unclassif ied
                                                                         22. PRICE
EPA Form 2220-1 (Rev. 4-77)   PREVIOUS EDITION is OBSOLETE
                                             331
                                                                  it US GOVERNMENT PRINTING OFFICE. 1981 -757-064/0252

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