;•:•:•: EPA-460/78-003 April 1978 EVALUATION OF THERMOSENSING DEVICES TO MEASURE DIURNAL FUEL TANK TEMPERATURE FOR IN-USE VEHICLE TESTING U.S. ENVIRONMENTAL PROTECTION AGENCY Office of Air and Waste Management Office of Mobile Source Air Pollution Control Emission Control Technology Division Ann Arbor, Michigan 48105 ------- EPA 460/3-78-003 EVALUATION OF THERMOSENSING DEVICES TO MEASURE DIURNAL FUEL TANK TEMPERATURE FOR IN-USE VEHICLE TESTING by Saip Ereren Olson Laboratories, Inc. 421 East Cerritos Ave. Anaheim, California 92805 Contract No. 68-03-2411 EPA Task Officer: Martin Reineman April 1978 ------- This report is issued by the Environmental Protection Agency to report technical data of interest to a limited number of readers. Copies are available free of charge to Federal employees, current contractors and grantees, and nonprofit organizations—in limited quantities—from the Library Motor Vehicle Emission Laboratory, Ann Arbor, Michigan 48105; or, for a fee, from the Na- tional Technical Information Service, 5285 Port Royal Road, Springfield, Virginia 22161. This report was furnished to the Environmental Protection Agency by Olson Laboratories, Inc. 421 East Cerritos Ave., Anaheim, California, 92805, in fulfillment of Contract No. 68-03-2411. The contents of this report are reproduced herein as received from Olson Laboratories, Inc. The opinions, findings, and conclusions expressed are those of the author and not necessarily those of the Environmental Protection Agency. Mention of company or product names is not to be con- sidered as an endorsement by the Environmental Protection Agency. Publication No. EPA-460/3-78-003 ------- FOREWORD Conducting a diurnal heat build for evaporative emission determination requires that the liquid fuel in the vehicle tank undergo a temperature excur- sion from 60 F to 84 F. Measuring the fuel temperature on certification vehicles is no problem, since the vehicles are supplied by the manufacturers with thermocouples permanently placed in the tank at the proper location. When conducting evaporative emission tests on in-use vehicles, thermocouple installation through the fuel cap presents leakage problems and the exact location of the thermocouple inside the fuel tank is not known. This task order was initiated to develop an indirect method of determining fuel liquid temperature by measurement of the fuel tanks's outer surface temperature. 111 ------- ABSTRACT Three fuel tanks were instrumented with different temperature sensors mounted at various external surface and internal volume locations. Three diurnal heat build tests were performed on each of the three tanks; two of the tanks being mounted on vehicles. All temperature readings were recorded simultaneously to determine which external sensor correlated best to the fuel temperature measured at the midpoint of the 40 percent volume fill. Resistance temperature detectors and grid thermocouples attached to the tank surface are substantially better indicators of internal fuel temperature than thermocouples mounted through the fuel cap. IV ------- CONTENTS Foreword iii Abstract iv Figures vi Conclusions 1 1. Introduction and Summary 2 2. Methodology 3 2.1 Selection of Temperature Sensors and Mounting Methods 3 2.2 Preparation of the EPA-Supplied Fuel Tank and Vehicle Fuel Tanks 4 2.3 Testing and Data Recording 4 3. Results and Discussion 8 4. Suggested Sensor and Mounting Technique 22 Appendices A. Data Formats A-l v ------- FIGURES Number 1 EPA Supplied Fuel Tank and Locations of the Temperature Sensors. - - 5 2 Vehicle Fuel Tank and Locations of the Temperature Sensors 6 3 Typical Fuel Tank Test 9 4 Fuel Tank Test No. 1 10 5 Fuel Tank Test No. 2 11 6 Fuel Tank Test No. 3 12 7 Typical Delta 88 Test 13 8 Delta 88 Test No. 1 14 9 Delta 88 Test No. 2 15 10 Delta 88 Test No. 3 16 11 Typical Impala Test 17 12 Impala Test No. 1 18 13 Impala Test No. 2 19 14 Impala Test No. 3 20 15 List and Description of Characters Used in Figures 3 through 14. .. 21 16 Diagrams of the Suggested Temperature Sensor and Magnet Holder for Mounting 23 VI ------- CONCLUSIONS The following conclusions are based on this project: o External sensors mounted on fuel tanks can be used to monitor the diurnal heat build when testing in-use vehicles for evaporative emissions. The readings from these sensors are closer to actual fuel temperature at midpoint of the 40 percent volume fill than readings from thermocouples routed through fuel caps. o Resistance temperature detectors (RTDs) and grid thermocouples gave the most satisfactory results among the external sensors. o Bead thermocouples mounted on tank surfaces are not reliable indicat- ors of internal fuel temperature. ------- Section 1 INTRODUCTION AND SUMMARY This final report is submitted by Olson Laboratories, to the Environmental Protection Agency (EPA) to document the conduct and findings of Task Order 4 of Contract No. 68-03-2411. The purpose of this task order was to develop an indirect method of determining fuel temperature using an external temperature sensor attached to the tank surface. After a review of technical literature, four types of temperature sensors were selected. One fuel tank supplied by the EPA and fuel tanks of two rented vehicles were instrumented with four Type J thermocouples (Iron-Constantan) located inside the tank at the 10 percent, 20 percent, 30 percent, and 70 percent fuel levels. A Type J thermocouple was routed through the fuel cap which was used on all three fuel tanks. This fuel cap was also equipped with a pressure tap. A set of each of the four types of sensors were mounted externally on the EPA-supplied fuel tank at the 20 percent, 40 percent, and 70 percent fuel levels. For the rental vehicles only, one of each of the four types of sensors was mounted externally at the 20 percent fuel level. Three diurnal heat build tests were conducted on each tank while venting the evaporative hydrocarbon emissions to atmosphere. All temperature data were recorded simultaneously with a digital printer of a datalogger. The data were then submitted in a punched card format defined by the EPA Project Officer. ------- Section 2 METHODOLOGY This section summarizes the methodology applied to instrumentation of fuel tanks with internal and external temperature sensors, testing, and data recording. 2.1 SELECTION OF TEMPERATURE SENSORS AND MOUNTING METHODS Technical literature was reviewed to determine the current state of the art in temperature measurement and to select four different temperature measure- ment sensors. Semiconductor temperature sensors were eliminated because of their limited sensitivity (approximately ±5 F) and the lack of commercial availability of necessary signal conditioning equipment. Strain gauge temper- ature sensors were eliminated because they are too fragile for this application. The four sensors originally selected for the project were: RTD, thermistor, c,rid thermocouple and bead thermocouple. These were selected because of their high sensitivity, ease of mounting, low cost, inexpensive signal conditioning requirements, and commercial availability. Type T thermocouples (Copper-Constantan) were used rather than Type J (Iron-Constantan). In the temperature range 50 F to 100 F, Type T thermocouples are superior to Type J since they are free of errors due to inhomogenity of wires. The four sensors which were actually used for the project and a description of the mounting techniques are summarized as follows: o Resistance Temperature Detector, by Omega Engineering, Inc. This is a 100 Ohm platinum sensor in which the temperature-sensitive platinum layer is separated from the medium to be measured by a thin ceramic substrate of high thermal conductivity. It was attached to tank surface with a permanent magnet. A small drop of epoxy under the magnet provided thermal insulation between the sensor and the magnet. A thin layer of thermally-conductive silicone compound (Z9 Silicone Super Heat Sink Compound by GC Elect- ronics) between the sensor and the tank surface ensured good thermal contact. A small piece of aluminized tape on the RTD provided a fixed location. o Type T Bead Thermocouple Soldered Onto the Tank Surface Thermocouple grade wires (20-gauge) were stripped about 1 centimeter and the two bare wires were twisted together. The tank surface was cleaned with sandpaper and then the thermocouple was soldered on the tank using 40/60 alloy, resin-core solder. The sensing tip was later insulated from the ambient air by a layer of epoxy. ------- o Type T Grid Thermocouple, by Hy-Cal Engineering The grid thermocouple is encased in two layers of kapton; one layer having pressure-sensitive adhesive backing. It was attached to the tank surface, then held in place firmly by aluminized tape. o Type T Thermocouple Bead Adhered to the Tank Surface In the plan of performance for this task order, a 5,000 Ohm thermistor by Omega Engineering, Inc., was proposed to be the fourth sensor. However, the signal conditioning units purchased for the thermistors were nonlinear in their voltage-versus-resistance relations. This created two nonlinearities to work with since the resistance-versus- temperature characteristics of thermistors are highly nonlinear. With the manufacturer's approval, the malfunctioning modules were returned. As a substitute for the thermistor, a Type T bead thermocouple was attached to the tank surface with thermally conductive adhesive (Thermal Bond 312, by Astrodyne, Inc.). 2. 2 PREPARATION OF THE EPA-SUPPLIED FUEL TANK AND VEHICLE FUEL TANKS One fuel tank was obtained as government-furnished equipment from the EPA, equipped with four internal Type J thermocouples mounted at the 10 percent, 20 percent, 30 percent, and 70 percent fuel levels and one Type J thermocouple routed through the fuel cap. A pressure tap was installed on the replacement fuel cap which provided an inexpensive and convenient way of measuring fuel tank vapor pressure. Three identical sets of each of the four selected sensors were externally mounted on the tank surface at 20 percent, 40 percent and 70 percent fuel levels (Figure 1). Two privately-owned vehicles, a 1977 Oldsmobile Delta 88 and a 1977 Chevrolet Impala, were also used for the tests. Fuel tanks of these vehicles were removed and four Type J thermocouples were installed on the sending units at the 10 percent, 20 percent, 30 percent, and 70 percent fuel levels. External sensors were mounted only at the 20 percent fuel levels of the two tanks (Figure 2). Undercoating on the fuel tank was removed and the exposed surface was cleaned before mounting the sensors. The same fuel cap with pressure tap and Type J thermocouple was used on all three tanks. 2.3 TESTING AND DATA RECORDING The EPA-supplied fuel tank and the fuel tanks of the two vehicles were filled to 40 percent of their total fuel capacity with Indolene unleaded test fuel chilled to 50 F. All tanks were tested three times in accordance with normal diurnal test procedures except that evaporative emissions were not measured. The internal 20 percent fuel level thermocouple was used to monitor the heat build manually. A Fluke 2240A Datalogger with a printer was used to record the data. The unit is programmed for thermocouple linearization and has a built-in cold junction compensation. Temperatures from the Type T and Type J thermocouples were read directly in degrees Fahrenheit. Linearized AP4151 modules by Action ------- 10% Fuel Leve"h, 0% Fuel Level Fuel Level uel Level. S e n d i n Type J Thermocouples Mounted inside the tank Pressure Tap Fuel Cap Thermocouple Identical Sets of Four Sensors Mounted on the Side of Tank Surface at Leve 1 s as Shown. Fuel Level/ Figure 1. EPA Supplied Fuel Tank and Locations of Temperature Sensors the ------- Type J Thermocouples Mounted on the Sending Unit 10% Fuel Level 20% Fuel Level 30% Fuel Level 170% Fuel Level Pressure Tap Fuel Cap Thermocouple 20% Fuel Level - Group of Four Sensors Mounted on the Side of Tank Surface at Level Indicated Figure 2. Vehicle Fuel Tank and Locations of the Temperature Sensors ------- Instruments Co., Inc., were used as signal conditioning for the RTDs. These units were calibrated to give 0 to 1 volt output for the temperature range 50 F to 100 F. The recorded voltage readings were converted into degrees Fahrenheit by using the equation: °F =50 (1 + Volts). All temperatures were recorded within 6 seconds, which was the time to scan and print out 18 channels. The datalogger was programmed to record the data in 2.5-minute intervals. A magnehelic pressure gauge with 0 to 1 inch water range and a water monometer with 0 to 30 inches water range were used to measure the fuel tank vapor pressure. ------- Section 3 RESULTS AND DISCUSSION The results of testing done for this task order can best be summarized by graphical presentation of data. The output of each external and internal temperature sensor is plotted against time for every diurnal test. Also, the deviation of the output of each external sensor at the 20 percent level from the actual fuel temperature at the same level versus time is plotted. These graphs are shown in Figures 3 through 14. The list of characters used and their description are given in Figure 15. The following conclusions can be drawn from these graphs. Surface temperatures measured by the RTD at the external 20 percent location are within ±2.0 F of the actual fuel temperature at that level. The grid thermocouple readings are within ±2.3 F of the internal temperature. Bead thermocouples do not give as satisfactory results as RTDs and grid thermocouples. Large thermal masses created by soldering and using adhesive might have caused the sluggish temperature response. Also, inherent danger in soldering to a fuel tank, long curing time for the adhesive, and questionable quality of the thermal contact achieved with the adhesive made bead thermocou- ples less desirable than RTDs and grid thermocouples. The thermocouple routed through the fuel cap is within ±4.2 F of the internal 20 percent fuel temperature. Both RTDs and grid thermocouples are superior to this sensor. Since it follows the internal fuel temperature more closely than the grid thermocouple and it can be easily mounted and recovered after testing, the RTD is preferred over the grid thermocouple. If the diurnal heat build procedure is modified so that the fuel temperature measured by an external RTD is monitored to rise from 61.0°F to 82.5 F within a 1-hour period, then the actual fuel temperature will follow the desired 60.0°F to 84.0°F heat build. The pressure readings observed were scattered over a wide range of values because the fuel cap could not be sealed properly. This might have affected the fuel vapor temperature but it should have no considerable effect on the fuel liquid temperature. ------- Figure 3. TYPICAL FUEL TANK TEST 10 IS 20 25 30 35 40 TIME (MINUTES) 45 SO SS 60 ------- l-t LO- CD UJ Q LU OC CL CC LU0 Q_ ' SI LU LUc\j Q ' en i LO I CD I Figure 4. FUEL TANK TEST NO. 1 10 15 20 25 30 35 M TIME (MINUTES) 45 SO 55 60 10 ------- Figure 5. FUEL TANK TEST NO. 2 —T— s T 1 55 10 IS 20 25 30 35 MO TIME (MINUTES) MS 50 60 11 ------- r- - to- co O UJ Q UJ QC CE QC LU0 Q_ ' 21 UJ LUfM Q ' Figure 6. FUEL TANK TEST NO. 3 LD I ,Q 10 IS 30 85 30 35 40 TIME (MINUTES) T 1 1 r- MS 50 55 60 12 ------- Figure 7. TYPICAL DELTA 88 TEST 10 IS 20 25 30 35 40 TIME (MINUTES) 45 50 55 60 13 ------- CD- tn- 3*- tn- UJ Q LU CC CL QC LU0 Q_ ' CL Q ' en i LO I Figure 8. DELTA 88 TEST NO. 1 10 15 20 25 30 35 40 TIME (MINUTES) 45 SO 55 60 14 ------- CO- U_ Q ' Figure 9. DELTA 88 TEST NO. 2 -1 1 1 1 1 1 1 —I I 1 I 1 SO 55 60 —I— 5 10 IS 20 25 30 35 4 TIME (MINUTES) 15 ------- r- - co- Figure 10. DELTA 88 TEST NO. 3 10 15 30 35 30 35 MO TIME (MINUTES) 45 50 55 60 16 ------- Figure 11. TYPICAL IMPALA TEST 10 IS 20 25 30 35 MO TIME (MINUTES) 45 SO 55 60 17 ------- co- co- UJ O , CM LU GC OL DC LU Q_ LU Q ' en i LO I to I . 0 Figure 12. IMPALA TEST NO. 1 10 15 80 35 30 35 40 TIME (MINUTES) 45 50 55 60 18 ------- UD- LU a: to i Figure 13. IMPALA TEST NO. 2 10 IS 20 25 30 35 40 TIME (MINUTES) 45 SO SS 60 19 ------- 10- LT>- cn i CD UJ Q DC ID- I— cc GC UJ0 Q_ « UJ en i in ID I Figure 14. IMPALA TEST NO. 3 0 S 10 IS 80 85 30 35 MO TIME (MINUTES) 45 SO 55 60 20 ------- CHARACTER USED DESCRIPTION A (TO) Ambient Temperature B (Tl) RTD (20% Fuel Level) E (T4) Bead Thermocouple, Soldered (20% Fuel Level) H (T7) Bead Thermocouple, Adhered (20% Fuel Level) K (T10) Grid Thermocouple (20% Fuel Level) N (T15) Fuel Cap Thermocouple P (T17) Internal Thermocouple (20% Fuel Level) R (T19) Internal Thermocouple (70% Fuel Level) B (Tl) - (T17) E (T4) - (T17) H (T7) - (T17) K (T10) - (T17) N (T15) - (T17) Figure 15. LIST AND DESCRIPTION OF CHARACTERS USED IN FIGURES 3 THROUGH 14 21 ------- Section 4 SUGGESTED SENSOR AND MOUNTING TECHNIQUE Sensor Resistance Temperature Detector by Omega Engineering, Inc., 100 Ohm platinum (0.00385 Ohms/Ohm/°C). Glass encapsulated platinum layer on a ceramic substrate. Dimensions of the Sensor 10.2 x 3.2 x 1.0 mm Mounting Technique A magnet with rubber holder is recommended to attach the sensor to fuel tank surface (Figure 16). A layer of silicone compound between the sensor and the tank surface provides a good thermal contact. Measuring Circuitry Linearized RTD Transmitter Module (AP4151) by Action Instruments Co., Inc. This unit operates directly off AC line power. It has zero and span adjustments. It accepts a three-wire RTD input for specified temperature ranges, and provides DC output proportional to the input temperature. Dimen- sions of the module are 8.7 x 5.9 x 4.3 cm. Approximate Price Sensor: $15.00 Linearized Transmitter Module: $195.00 22 ------- Figure 16. DIAGRAMS OF THE SUGGESTED TEMPERATURE SENSOR AND MAGNET HOLDER FOR MOUNTING Sensor Knob Retaining Screw Hand!ing Knob Tank Surface Sensor Silicone Layer Rubber 23 ------- Appendix A DATA FORMATS ------- DATA FORMATS COLUMN NO. 1 2-3 DESCRIPTION Task Order No. Card No. 4-5 6 7-8 9-14 15 16 17-19 20-21 22-24 25-27 28-30 31-33 34-36 37-39 40-42 43-45 46-48 49-51 52-54 55-57 58-60 61-63 64-66 67-69 70-72 73-75 76-78 Project Code Contract Code Site Date Vehicle Test No. Time Elapsed Desired Fuel Temperature Pressure (TO) Ambient Temperature (Tl) RTD (20% Level) (T2) RTD (40% Level) (T3) RTD (70% Level) (T4) Bead Thermocouple, Soldered (20% Level) (T5) Bead Thermocouple, Soldered (40% Level) (T6) Bead Thermocouple, Soldered (70% Level) (T7) Bead Thermocouple, Adhered (20% Level) (T8) Bead Thermocouple, Adhered (40% Level) (T9) Bead Thermocouple, Adhered (70% Level) (T10) Grid Thermocouple (20% Level) (Til) Grid Thermocouple (40% Level) (T12) Grid Thermocouple (70% Level) (T15) Fuel Cap Thermocouple (T16) Internal Thermocouple (10% Level) (T17) Internal Thermocouple (20% Level) (Monitor Channel) (T18) Internal Thermocouple (30% Level) (T19) Internal Thermocouple (70% Level) COMMENTS 4 Time (Minutes) Card No. 0.0 2.5 60.0 1 2 25 77 4 07 YYMMD Vehicle NO. 0 1 2 EPA Fuel Tank Delta 88 77 Impala Minutes °F Inches Water °F °F °F °F o o o o o o o o o o o el) ° F F F F F F F F F F F F °F o F FORMAT 11 12 12 11 12 16 11 11 F4.1 12 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 F4.1 A-l ------- TECHNICAL REPORT DATA (Please read Instructions on the reverse before completing) 1. REPORT NO. EPA-460/78-003 3. RECIPIENT'S ACCESSION-NO. 4. TITLE AND SUBTITLE EVALUATION OF THERMOSENSING DEVICES TO MEASURE DIURNAL FUEL TANK TEMPERATURE FOR IN-USE VEHICLE TESTING 5. REPORT DATE APRTT. 1Q7« 6. PERFORMING ORGANIZATION CODE 7. AUTHOR(S) SAIP EREREN 8. PERFORMING ORGANIZATION REPORT NO 9. PERFORMING ORGANIZATION NAME AND ADDRESS OLSON LABORATORIES, INC. 421 EAST CERRITOS AVENUE ANAHEIM, CALIFORNIA 92805 10. PROGRAM ELEMENT NO. 11. CONTRACT/GRANT NO. 68-03-2411 12. SPONSORING AGENCY NAME AND ADDRESS U.S. ENVIRONMENTAL PROTECTION AGENCY OFFICE OF AIR AND WASTE MANAGEMENT EMISSION CONTROL TECHNOLOGY DIVISION ANN ARBOR, MICHIGAN 48105 13. TYPE OF FtEPORT AND PERIOD COVERED 14. SPONSORING AGENCY CODE EPA-ORD 15. SUPPLEMENTARY NOTES 16. ABSTRACT Three fuel tanks were instrumented with different temperature sensors mounted at various external surface and internal volume locations. Three diurnal heat build tests were performed on each of the three tanks; two of the tanks being mounted on vehicles. All temperature readings were recorded simultaneously to determine which external sensor correlated best to the fuel temperature measured at the midpoint of the 40 percent volume fill. Resistance temperature detectors and grid thermocouples attached to the tank surface are substantially better indicators of internal fuel temperature than thermocouples mounted through the fuel cap. 17. KEY WORDS AND DOCUMENT ANALYSIS DESCRIPTORS b.IDENTIFIERS/OPEN ENDED TERMS c. COSATl Field/Croup !? DISTRIBUTION STATEMENT \ RELEASE TO PUBLIC 19. SECURITY CLASS {This Report) UNCLASSIFTKD 20. SECURITY CLASS (Tills pa:X) UNCLASSIFIED 21. NO. OF PAGES 32 22. PRICE ------- |