United States
Environmental Protection
Agency
Office of
Emergency and
Remedial Response
EPA/ROD/R02-87/052
September 1987
Superfund
Record of Decision:
South Brunswick, NJ
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* TECHNICAL REPORT DATA
'fleast read Inttruenons on tHt went btfort
NO.
EPA/ROD/R02-87/052
3.
3 RiCi"6NT s ACCESS.CN NO
SUPERFUND RECORD OF DECISION
South Brunswick Landfill, NJ
Second Remedial Action - Final
OATf .
September 30, 1987
»€R*ORMING ORGANIZATION COO€
. HR0ORMING ORGANIZATION RgPQRT SO
SS
10. PROGRAM ILCMJNT NO
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DECLARATION STATEMENT
RECORD OF DECISION
BROWNING-FERRIS INDUSTRIES SOUTH BRUNSWICK LANDFILL
SITE LOCATION;
The Browning-Ferris Industries South Brunswick Landfill Site
is located along New Road approximately one-half mile north-
west of U.S. Route 1 in Middlesex County/ New Jersey.
STATEMENT OF PURPOSE:
This decision document represents the selected and implemented
remedial action for this site evaluated in the context of
CERCLA, as amended by SARA/ and to the extent practicable/
the National Contingency Plan.
The State of New Jersey has concurred on the selected remedy.
DESCRIPTION OF THE SELECTED REMEDY;
The site strategy for the BFI-South Brunswick'Landfill is on-site
containment and monitoring for a period of thirty (30) years.
A post remedial monitoring plan has been proposed to assess
the long term integrity of the remedy and evaluate any previous
off-site migration of contaminants in the context of chemical /•
specific/ambient ARARS. Should the monitoring program reveal
exceedances of ARARS/ additional remedial action will be
considered.
The remedial action consists of a leachate collection/treatment
system/ slurry wall, clay cap and gas venting system. The
remedial work was initiated in May, 1983 and was completed in
September, 1985. In addition, EPA has determined that a fence
should be installed along the site perimeter to restrict access/
eliminate any nuisance threats and preserve the integrity of
the remedial action.
DECLARATION;
The selected remedy is protective of human health and the environ-
ment/ attains Federal action and location specific requirements
that are applicable.or relevant and appropriate and is cost-
effective. *>• *
^.
A State landfill capping requirement has been waived since
the containment system in- place provides an equivalent level of
performance. ' 4
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The Statutory preference for treatment is not satisfied
because treatment was found to be impracticable.
The remedy was selected on the basis of its implementability and
proven effectiveness in landfill containment given the hydrogeology
of the site, size of the landfill and waste disposal practices.
The landfill accepted predominantly municipal refuse which
was comingled with hazardous waste. Excavation and off-site
disposal and/or treatment of hazardous waste was not considered
feasible or cost-effective due to the size of the landfill
and the fact that discrete areas of hazardous waste disposal
could not be adequately identified.
.7#-
Date ^ Christfepher^J. D^dgett
Regional Administrator
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SUMMARY OF REMEDIAL ALTERNATIVE SELECTION
BROWNING-FERRIS INDUSTRIES SOUTH BRUNSWICK LANDFILL
SOUTH BRUNSWICK, NEW JERSEY
SITE LOCATION AND DESCRIPTION
The Browning-Ferris Industries (BFI) South Brunswick Township
Landfill is located along New Road approximately one-half mile
northwest of U.S. Route 1 in Middlesex County, New Jersey
(Figure 1). .
The landfill occupies an area of approximately 68 acres. A
significant portion of the land surrounding the site is wooded.
A private residence is located adjacent to the site, a school and
park are located directly across New Road and a housing development
has been constructed north of the site.
The site is in close proximity to Heathcote Brook which is -a
tributary to the Millstone'River. The City of New Brunswick
occasionally draws water for drinking from an intake 10 miles
downstream. Groundwater flows in a south-easterly direction and
the nearest public groundwater supply is located approximately 1
mile north of the site. '
SITE HISTORY.
The site/ which operated for more than twenty years as a solid
waste landfill/ accepted municipal refuse/ pesticides/ chemical
wastes and hazardous wastes. Title to the South Brunswick
Landfill property was acquired by Princeton Disposal Service/
Inc./ predecessor in interest to BFI of South Jersey/ Inc./
on or about May 31, 1973, from G & J Spilatore Excavation/
previous owner and operator of the facility. The landfill was
registered with the New Jersey Department of Environmental Protection
(ttJDEP) on August 19/ 1970. Pursuant to a closure order from the
NJDEP on July 24, 1978, the site was officially closed on December
31, 1978.
In June, 1980 the U.S.. Environmental Protection Agency (EPA)
conducted an investigation of the BFI-South Brunswick Landfill
site. The sampling results revealed elevated levels of volatile
organic compounds in seven on-site monitoring wells as well as
five on-site surface water sampling locations. The data from
this sampling effort resulted in the site being included on the
Superfund National*Priorities List in December/ 1982. The comp-lete^k
chemical data base from this investigation is provided in Appendix ^V
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FIGURE 1.
Vo ..a
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UTH
LAN
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B
1
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Monmoutfa
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-3-
ENFORCEMENT ACTIONS
Browning-Ferris Industries of South Jersey, Inc., as the owner and
operator of the landfill since 1973, was identified by EPA as a
responsible party with respect to the site. Accordingly, EPA
entered into negotiations with the company and on April 5, 1982,
EPA and BFI entered into an agreement concerning remedial efforts
to be performed at this site. The agreement was in the form of
a Resource Conservation and Recovery Act (RCRA) 7003 Administrative
Order on Consent (Index No. RCRA-700320101) which outlined a
three-phase work program.
Phase I consisted of a hydrogeologic investigation designed to
determine the nature and extent" of contamination related to the
site. This work was performed by Wehran Engineering as consultant
to BFI in the summer of 1982. . -
Phase II called for development of a Remedial Plan and construct-
ion of the EPA-selected remedy. The Remedial Plan which was
submitted to EPA in February, 1983 consisted of a leachate
collection/treatment system, slurry wall, clay cap and gas venting
system. The remedial work was initiated in May, 1983 and was
completed in September, 1985.
Phase III, a post-remedial environmental monitoring program designed
to provide a continuous assessment of the long-term effectiveness
of the completed on-site remedial action, was proposed by BFI on
June 5, 1987. It is anticipated that BFI will implement this progr'
under EPA supervision, beginning in the fall of 1987.
HYDROGEOLOGIG INVESTIGATION
The Hydrogeologic Investigation revealed that the majority of
the site is underlain by a dense unfractured diabase bedrock with
an estimated average permeability of 1 x 10~7 cm/sec. The bedrock
is overlain by a low permeability (10~6 to 10~7 cm/sec) satfrolite or
residual soil. Groundwater occurs primarily within an unconfined
water table zone within the landfill refuse and Raritan formation.
Groundwater flow in this unconfined zone is predominantly lateral
and southerly to groundwater discharge points south of the site
(proximate streams and seepage areas).
In a small portion of the site along the northern boundary, the
bedrock was found to be fractured and of much greater permeability
(2 x 10~4 to 4 x 10~6 cm/sec). Observed groundwater elevations
indicated upward vertical gradients within the bedrock. Thus,
contaminants were not expected to flow through the bedrock in any
significant quantities.
The Hydrogeologic Investigation supported the findings of EPA's
June, 1980 sampll-stj effort. The groundwater in the shallow
unconfined aguifer was found to be contaminated with total
organics (TVO's) ranging from 80 to 1,955 parts per billion
Groundwater in the deeper fractured bedrock zone in the northern
portion of the site was also found to be contaminated with TVO's,
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-4-
ranging from 23 to 494 ppb. Elevated levels of iron were also
detected in both the shallow and fractured bedrock on-site moni-
toring wells. In general, the highest concentrations of ground- •
water contamination was found in the surficial unconfined aquifer.
A resistivity survey was used in conjunction with analyses of
indicator parameters in off-site monitoring wells in order to
determine the relative extent of off-site migration of contaminants.
Results showed that with two exceptions, the contaminants appeared
to be restricted immediately along the margin of the landfill.
At two locations along the western edge of the landfill, it was
apparent that leachate had flowed radially from the landfill over
the ground surface toward a small stream located approximately
1000 feet west of the site. Leachate flow- was evidenced by
ground staining and varying amounts of vegetative stress.
The groundwater data obtained during the hydrogeologic investi-
gation is provided in Appendix 1. .
The results of the June, 1980 EPA sampling effort and the BFI
hydrogeo-logic Investigation revealed that leachate eminating from
the landfill was degrading surface and groundwater guality in the
vicinity of the site. Although the site posed no immediate threat
to potable water supplies, there was concern about potential future
impacts on regional groundwater quality. Uncontrolled radial
flow of leachate from the landfill posed a threat of direct contact
to human health and the environment. Therefore, EPA determined
it was necessary to implement a remedial action which would
mitigate any further release of contamination from the landfill,
CURRENT SITE STATUS
The selected containment remedy for the BFI South Brunswick Land-
fill has been in place and operational since September, 1985.
This Record of Decision (ROD) evaluates the remedy selection
process in the context of the Superfund Amendments and Reauthori-
zation Act of 1986 (SARA). EPA believes the site has been effectively
remediated, thereby mitigating the threat of release of contaminants
into the environment which could present an imminent and substantial
endangerment to human health and th.e environment.
The operational success of the remedy is evidenced by monthly
analysis of leachate (quantity and quality) discharged to the
Stony Brook Regional Sewerage Authority for treatment. ' The
volumetric leachate discharge rate for the 68 acre site has been
reduced from an average of 150,000 gallons/day prior to remediation,
to a current average of 20,000 gallons/day. Furthermore, water
quality analysis «Qf lejachate has revealed an improvement in
leachate quality over time. Leachate quality and volumetric
discharge data is provided in Appendix 4.
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-5-
Visually there has been a marked benefit to the surrounding envir-
onment as a result of the completed remedial activities. Prior to
remediation, proximate streams and wetlands were fouled with leach-
ate migrating laterally from the site. Presently, there is no
visual evidence of leachate entering adjacent surface waters.
ALTERNATIVES EVALUATION
Based upon information gathered during the Hydrogeologic Investi-
gation, a range of containment alternatives involving a leachate
collection system, slurry wall and clay cap, were developed to
control the release of hazardous substances emanating from the
landfill. Specifically, remedial alternatives were developed
to address the findings and conclusions outlined below.
A. The majority of the site was found to be underlain by low
permeability diabase bedrock and/or residual soil which
would provide a suitable strata to "key-in" a slurry wall.
B. The northern portion of the site where fractured bedrock was
encountered would not provide a suitable "key in" strata.
C. Leachate flow in the unconfined water bearing zone was pre-
dominantly lateral, hence a perimeter collection/containment
system would control off-site leachate migration.
D. Capping and proper grading of the landfill with low perme-
ability clay would control drainage, reduce infiltration and
thereby reduce leachate generation to a minimum.
E. A collection system designed to provide a preferential
hydraulic gradient towards the collection line within the con-
fines of a slurry wall would eliminate radial leachate
discharges from the site and reduce the hydraulic head
within the landfill.
F. A low permeability clay/soil slurry wall keyed into a
suitable bottom strata would reduce to a minimum the flow of
groundwater through the site.
The hydrogeologic characteristics of the site were found to be very
conducive to site containment. Accordingly, eight (8) containment
options and the option of taking no action were evaluated. The
following is a comparative summary of each alternative.
(1) NO ACTION
The no action alternative included the construction of a security
fence to restrict^, access to potentially .contaminated areas and the
implementation of a long-term.groundwater monitoring program to
provide advance warning of increased future releases of hazardous
substances from the landfill into the environment. This alternative
was considered inappropriate as a permanent remedy since it would
not adequately protect human health o» mitigate any releases or
potential releases-of—contaminants into the environment.
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-7-
treated would also be reduced to a practical minimum. Once again,
the major disadvantage asssociated with this alternative was the
"open container effect", as is described above. In addition,
since residual soils are somewhat more permeable than the under-
lying bedrock, the potential for migration of contaminated ground-
water was greater than with the deeper bedrock slurry wall.
(7) SLURRY VJALL TO RESIDUAL SOIL, CLAY CAP, NO LEACHATE COLLECTION
SYSTEM
This alternative is very similar to the construction of a slurry
wall keyed into bedrock and a clay cap as described in Alternative
(5). Again, the "open container" effect would be minimized by
the installation of a clay cap. However, since, in this alterna-
tive, the slurry would be keyed into residual soil, which is'more
permeable than bedrock, there would be a greater potential for
groundwater migration beneath the wall.
(8) SLURRY WALL TO RESIDUAL SOIL AND BEDROCK, CLAY CAP, AND NO
. LEACHATE COLLECTION SYSTEM
In this case alternatives 5 and 7 are combined to provide slurry
wall key-in to bedrock where it is relatively shallow with the *
transition to residual soil where the bedrock deepens. By allowing
for two key-in materials, excessive depths on slurry wall construc-
tion where key-in is to bedrock would be eliminated and construction
costs reduced. The construction of this slurry wall in conjunction
with a clay cap would minimize leachate formation, off-site leach-
ate migration and long-term leachate handling and treatment. The
"open container" effect would once again be minimized but long-term
leachate buildup within the landfill could be a significant
problem without the benefit of a leachate collection system. The
portion of the slurry wall which would be keyed into residual
soil, which is more permeable than bedrock, could also be of
concern since this would provide for a greater potential for
groundwater migration beneath the wall.
(9) SLURRY WALL TO RESIDUAL SOIL AND BEDROCK, CLAY CAP WITH GAS
VENTS AND LEACHATE COLLECTION SYSTEM
In this case the slurry wall design would be identical to Alterna-
tive (8). The wall key-in would be to bedrock where it is relatively
shallow with a transition to residual soil where the bedrock
deepens. The construction of a slurry wall, clay cap and gas
vents would minimize leachate formation, off-site leachate migration
and treatment and gas pressure build-up within the landfill. The
"open container" effect is reduced to a minimum and any leachate
buildup would be collected and pumped to the Stony Brook Regional
Sewerage Authority for treatment by the leachate collection
system. Thus, ttfe^af*ge leachate volumes formed from rainwater
infiltration through the landfill and associated treatment
costs would be significantly reduced with the construction of
clay cap and leachate collection system. The portion of the slurry.
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-8-
wall keyed into residual soil would be of less concern here
because of the leachate collection syscem which would reduce the
level of groundwater within the landfill to create a preferential
hydraulic gradient into the containment system.
After a careful evaluation of these nine (9) Alternatives, EPA
decided that the most cost-effective and environmentally sound
remedy was Alternative (9).
It is important to remember that the evaluation, selection and
implementation of the selected remedy occurred prior to the new
administrative requirements of SARA. Therefore, the new SARA
evaluation criteria for remedy selection, (i.e., permanence,
innovative technologies and consistency with applicable or
relevant and appropriate requirements (ARARs) of other environmental
laws) were not formally addressed in the original 1983 remedy
selection process. Since this is the first ROD written for the
BFI-South Brunswick Landfill site, the purpose is to evaluate the
remedy selection process in the context of CERCLA, as amended by
SARA.
Table 1 provides a summary of each alternative in the context of
the SARA evaluation criteria.
SELECTED REMEDY
The site strategy for the South Brunswick Landfill is onsite
containment and monitoring for a period of thirty (30) years.
Should the post remedial monitoring program reveal exceedences of
ambient or chemical specific ARARs for air, surface water and
groundwater, additional remedial action may be required. However,
EPA believes that the completed on-site containment system is
functioning as designed to eliminate contaminant migration from
the site.
DESCRIPTION OF SELECTED REMEDY
The following is a detailed description of the selected remedy:
SLURRY WALL
A clay/soil slurry wall has been constructed along the site peri-
meter excluding the northern portion of the site where the bedrock
is known to be fractured. The slurry wall has been located in a
conservative position so that the entire area enclosed by the
slurry wall is underlain by low permeability diabase and/or
residual soil. This slurry wall provides key-in to bedrock where
it is relatively shallow with a transition to residual soil where
the bedrock deepens* ^"or the majority of the slurry wall (7315
ft in length) alignment, the key-in is to bedrock (63%). The
remaining 37% of the slurry wall length is keyed into residual
soil.
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"SUMMARY OP ALTERNATIVES IN
SARA EVALUATION CRITERIA
TABLE
ALTERNATIVE
2
LEACHATE
COLLECTION
SYSTEM*,
NO CAP, AND
NO SLURRY
NALL
ALTERNATIVE
3,.
LEACHATE
COLLECTION
SYSTEM*,
CLAY CAP, AND
NO SLURRY
NALL
ALTERNATIVE
4
SLURRY HALL
TO BEDROCK,
NO CAP AND
NO LEACHATE
COLLECTION
SYSTEM
ARAR'SS
LOCATION
AND
ACTION
SPECIFIC
Does not
comply with
R^RA closure
requirements;
Complies with
Clean Water Act
discharge to
POTW require-
ments ***
Compliance with
Federal RCRA
closure
requirements
and Clean Water
Act discharge
to POTW
Does not comply
with RCRA
closure
requirements
REDUCTION
OF
TOXICITY,
MOBILITY,
OR
VOLUME
VIA
TREATMENT
Treatment of
volatile
organics at
POTW
*
SAME AS ABOVE
"
NO REDUCTION
SHORT
TERM
EFFECTIVENESS
•
Risk
Reduction-low
Short-term
Risks due to
Construct ion-
- low
Risk
Reduction-
moderate
Short-term
Construction
Risks-low
Risk
Reduction-low
Short-term
Construction
Risks-Mod.
LONG TERM
EFFECTIVENESS
AND
PERMANENCE
Residual
Risks-high
OfcM-high
Human Exp.-
moderate
Long-term
Reliability-
low
Residual
Risks-Mod.
OfM-high
Human Exp.-
moderate
Long-term
Reliability-
moderate
Residual
Risks-high
O&M-low
Human Exp.-
moderate
Long-term
Reliability-
moderate *
IMPLEMENT-
ABILITY
Easily
constructed.
Will operate
reliably !
Discharge to
POTW— permit
needs to be
obtained
Treatment
capacity
available
SAME AS ABOVE
Easily
constructed.
Will operate
reliably.
,
COST
Capital-low ,
« ' >
O&M-high
Five Year
Review-high
Potential
Future RA
Costs-high
Capital-Mod.
O&M-moderate
Five Year
Review-high
Potential
Future RA
Costs-Mod.
Capital-Mod.
O&M-low
Five Year
Review Costs-
Potential
Future RA
Costs-high
OVERALL
PROTECTION
OF PUBLIC
HEALTH AND
THE
ENVIRONMENT
Does not provide
adequate protection
of human health 'and
the environment
i
SAME AS ABOVE
SAME AS ABOVE
•
;
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TABLE 1 PAGE 2
-
ALTERNATIVE
5
SLURRY WALL
TO BEDROCK,
CLAY CAP AND
NO LEACHATE
COLLECTION
SYSTEM
,
ALTERNATIVE
6*
SLURRY (ALL
TO RESIDUAL
SOIL,NO CAP
AND NO
LEACHATE
COLLECTION
SYSTEM
ALTERNATIVE
7
SLURRY (ALL
TO RESIDUAL
SOIL, CLAY
CAP AND NO
LEACHATE
COLLECTION
SYSTEM
ARAR'SI
LOCATION
AND
ACTION
SPECIFIC
Compliance with
Federal RCRA
cjpaure
requirements
fc
Same as
Alternative 4
Same as
Alternative 5
OF
TOXICITY,
MOBILITY,
OR
VOLUME
VIA
TREATMENT
NO REDUCTION
•
NO REDUCTION
NO REDUCTION
SHORT
TERM
EFFECTIVENESS
Risk
Reduction-
moderate
Short-term
Construction
Risks-Mod.
Risk
Reduction-low
Short-term
Construction
Risks-Mod.
-
Same as
Alternative 5
LONG TERM
EFFECTIVENESS
AND
PERMANENCE
Residual
Risks-Mod.
OUt-low
Human Exp.-
low
Long-term
Reliability-
moderate
Residual
Risks-high
OUt-low
Human Exp.-
moderate
Long-term
Reliability-
moderate
Residual
Risks-Mod.
Out-moderate.
Human Exp.-
low
Long-term
ReliaUlity-
IKXk^B)
•^ '*
IMPLEMENT-
ABILITY
'
Easily
constructed.
Will operate
reliably.
SAME AS ABOVE
SAME AS ABOVE
•
COST
Capital-Mod.
OUt-low
Five Year
Review-high
Potenial
Future RA
Costs-Mod.
Capital-low
OUt-low
Five Year
Review-high
Potential
Future RA
Costs-high
Capital-Mod.
O&M-moderate
Five Year
Review-high
Potential
Future RA
Costs-Mod.
OVERALL
PROTECTION
OF PUBLIC
HEALTH AND
THE
ENVIRONMENT
• '
1
SAME AS ABOVE
SAME AS ABOVE
SAME AS ABOVE
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PAGE 3
ALTERNATIVE
8
SLURRY WALL
TO RESIDUAL
SOIL AND BED-
ROCK, CLAY CAP
AND NO LEACH-
ATE COLLECTION
SYSTEM
ALTERNATIVE
9
SLURRY UjtLL TO
RESIDUAL SOIL
AND BEDROCK,
CLAY CAP AND
A LEACHATE
COLLECTION
SYSTEM*
(CHOSEN ALT.)
ARAR'st
LOCATION
AND
ACTION
SPECIFIC
Compliance with
Federal RCRA
closure
requirements
Compliance
with Federal
RCRA closure
requirements
and Clean Water
Act discharge
to POTW
requirements
REDUCTION
OF
TOXICITY,
MOBILITY,
OR
VOLUME
VIA
TREATMENT
NO REDUCTION
••'
Treatment of
volatile
organics at
POTW
SHORT
TERM
EFFECTIVENESS
Risk
Reduction-
moderate
Short-term
Construction
Risks-Mod.
Risk
Reduction-
high
Short-term
Construction
Risks-Mod.
LONG TERM
EFFECTIVENESS
AND
PERMANENCE
Residual
Risks-Mod.
out-moderate
Human Exp.-
low
Long-term
Reliability-
moderate
Residual
Risks-low
OfiM-moderate
Human Exp.-
low
Long-term
Reliability-
high
IMPLEMENT-
ABILITY
Easily
constructed.
Will operate
reliably.
Easily
Constructed
Will operate
reliably
Available POTW
capacity
COST
Capital-Mod.
Ottt-Mod.
Five Year
Review-high
Potential
Future RA
Costs-Mod.
Capital-high
O&M-high
Five Year
Review-high
Potential
Future RA
Costs-low
OVERALL
PROTECTION
OF PUBLIC
HEALTH AND
THE
ENVIRONMENT
i
•
SAME AS ABOVE
i
Adequate protection
of human health and
the environment is
provided.
* Includes leachate treatment at Publicly Owned Treatment Works (POTW).
** The No Action alternative would not meet ARAR's, reduce toxicity, mobility or volume of contaminants,
provide short or long-term effectiveness and be protective of human health and the environment.
*** AS discussed on p. 19, State capping requirements are not met by any of the above alternatives although
equivalent performance is achieved by Alternative 9.
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-12-
Where the cut-off wall is keyed into the bedrock, inflow through
beneath the wall are considered negligible. Where the wall is
into the residual soil, inflow from outside of the wall will exist
commensurate with the permeability of the saprolite. Inflow, as
opposed to outflow, will result from the induced gradient developed
by the leachate collection line.
Construction of the slurry wall was of the slurry trench clay type.
The wall is designed to achieve a permeability of 1.0 x 10"7
cm/sec. The slurry wall is a minimum of three feet in thickness.
Slurry wall permeability testing was performed in place durinq
construction to confirm compliance with design specifications.
CAPPING AND SITE GRADING
A multi-layer clay cap designed to facilitate surface runoff and
prevent infiltration was constructed over the entire site, including
the area underlain by fractured bedrock. Reduction of surface
infiltration through the landfill will significantly reduce long
term leachate generation. The detail of the final cover is shown
in Figure 2. The cap consisted of the following:
- Twelve inches of clay soil compacted to achieve a maximum
permeability of 1.0 x 10~7 cm/sec.
- Six inches of sandy soils (well-drained) to provide
subdrainage of the clay and minimize the occurance
of saturated conditions which could harm vegetative
cover.
- Six inches of soil suitable to sustain vegetative growth
seeded and fertilized in accordance with the recommendations
of the local unit of the Soil Conservation Service.
The above-described cap is in compliance with RCRA action-specific
ARAR's (Table 2 of Appendix 2).
LEACHATE COLLECTION SYSTEM
The leachate collection system consists of the following elements:
0 A gravel packed perimeter collection line
0 Gravel packed interior collection lines
0 Access/maintenance manholes spaced a maximum of 500 feet on
center
0 Intermediate pump stations
*%« *
The collection system inside of the perimeter slurry wall is
designed to intercept groundwater flow within the unconfined water
bearing zone. The perimeter collection line has been constructed
to induce a hydraulic gradient which facilitates the flow of ground-
water towards the collection lines, the line consists of a six-
inch perforated pipe within a granular drainage aggregate and
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."•'*'
t >
vm • •&« .^^B ^B.^^. ^& A&_* s* ~:1»V_" * .. • _ -^^^"^^^ . '
-* • . . '. . • . *. • ?r ",
-:W^a^
FINAL COVER DETAIL
Figure 2
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-14-
fliter fabric envelope. The height and depth of the collection
line are dependent upon the required slopes for proper drainage
and the flow net developed within the unconfined water table. The
collection line conveys leachate to two pumping stations which pump
leachate to the central metering station, which then discharges to
the New Road sewer line and, ultimately, to the Stony Brook Regional
Sewerage Treatment Plant. The collection line has also been
designed with access manholes throughout the system. This allows
for inspection, maintenance, and repair of the facilities as
necessary. The leachate collection system and cut-off wall are
illustrated in Figure 3.
GAS VENTING SYSTEM
With the construction of a relatively impermeable cap, vertical
venting of landfill gases was necessary to minimize the potential
for methane gas buildup within the landfill. A series of permeable
gas ducts were constructed throughout the top of the main fill areas.
Since gases can be present in high concentrations in the vents,
a fence was installed to control access. Landfill gases are also
vented from manhole covers providing access to the leachate collection
system every 500 feet along the perimeter of the landfill.
FENCING
EPA has determined that a fence should be installed along the site
perimeter to restrict access, eliminate any nuisance threats and
ensure the integrity of the remedial action.
POST REMEDIAL MONITORING
A post remedial off-site monitoring program has been proposed by
BFI and submitted to EPA and NJDEP for review. The purpose of
the monitoring program is to evaluate the effectiveness of the
completed remedial action for a period of thirty years and assess
the impacts of any pre-remedial off-site migration of contaminants.
The program sets forth plans and methodologies for implementing
the following!
• Installation of groundwater monitoring wells along the peri-
meter of the site,
• Sampling and analysis of groundwater, surface water and sedi-
ments and air,
• Measuring hydraulic gradients along the slurry wall,
0 Identification of State and Federal ambient and chemical
specific ARARf*' «•
0 Investigate any potential off-site soil contamination related
to previous off-site leachate migration
A more detailed discussion of the .monitoring program is provided
in the following subsections. However, EPA may modify the monitoring
-------
Figure 3
35* WIDE WORK PLATFORM FOR SLURRY MILL i
I MM 2* TNCN I
COMPACTED aAV OR
•SLURRY CUT-OFF WALL
10 BEDROCK
IMPERVIOUS CAP AND FINAL
COVER
C
fjf/sr i
FILL
KEY-IN TO PRACTICAL
OCPTM
OR MAX SAFE SLOfO
_ ^w ••• '' - •• •• ^ ••••«»• ^tf
i \ \l« mrtR FABRIC
fTOPOFUABASE
' f HOPE OR PVC OBCMARGEUNE
FROM PUMP STATION
__ I FR
CLAY HALL I DUE TO CONSmuCTAMLITYl -» ^—*' *"N WOTM FOR SUJRRV
-------
-16-
program (e.g. sampling locations, parameters and frequency) as
necessary in order to fully evaluate the remedy's protectiveness of
human health and the environment.
Groundwater Monitoring
The post-remedial groundwater monitoring network will contain
thirteen monitor wells. Three of these monitor wells (BR-1, BR-2
and BR-3) will be completed in the fractured bedrock underlying
the northern portion of the site and ten wells (RF-1 through RF-10)
will monitor groundwater quality in the more shallow Raritan
Formation sediments. The three bedrock wells to the north will
also address the elevated level of total volatile organics discov-
ered in the area during the pre-remedial action Hydrogeologic
Investigation. The thirteen monitoring wells will be positioned
approximately 500 feet apart along the entire perimeter of the site
and will be sampled initially on a quarterly basis for two quarters.
Groundwater samples will be analyzed for all Priority Pollutants
plus up to 40 additional parameters. After data from both sampling
events has been reviewed, future sampling frequencies and parameters
will be specified.
surface Water and Sediment Sampling
One upstream and two downstream surface water and sediment sampling
stations will be established by the EPA based upon field observations,
Surface water and sediment samples will be collected on a quarterly
basis for two quarters at the same time the ground water monitor
wells are sampled. Each sample will be analyzed for the Priority
Pollutants plus up to 40 additional parameters. After the data
from the first two sampling events has been reviewed, modifications
to the surface water and sediment sampling program will be specified.
Off-site Soil Sampling
Soil sampling locations to assess areas of potential residual
contamination related to previous off-site leachate migration will
be determined by EPA based upon field observations. Soil samples
will be analyzed for priority pollutants plus up to forty additional
parameters.
Air Sampling and Analysis
The post-remedial air pollution control monitoring program will
include two initial events: point source emissions testing and
ambient air qualtey«mcrhitoring. These two events will be conducted
in accordance with the protocols approved by EPA with the consul-
tation of NJDEP. After the data from the point source testing
and ambient air quality monitoring have been reviewed, future
sampling frequencies and parameters wjj.1 be specified.
-------
-17-
Leachate Collection System Monitoring
The.purpose of the leachate monitoring program is to verify that
leachate is not building up inside the slurry wall. In order to
be assured that any groundwater migration is into the containment
system, it is necessary to maintain a lower water level within
the landfill. Groundwater levels inside and outside of the
perimeter slurry wall will be monitored using leachate collection
system manholes and groundwater monitoring wells, respectively.
In addition to the Post-remedial Environmental Monitoring Program,
Section 121(2)(c) of SARA requires EPA to review remedial actions
that result in any hazardous substances, pollutants, or contaminants
remaining at the site no less often than each five (5) years
after the initiation of such remedial action, to assure that human
health and the environment are being adequately protected. If
upon such review, it is the judgment of EPA that further remedial
action is appropriate at this site, the EPA will implement, or
through enforcement action require that such action be implemented.
»
OPERATION AND MAINTENANCE
Operation and maintenance is required to ensure the continued
effectiveness of the remedial action. Aspects of operation and
maintenance can generally be classified as follows:
0 Scheduled inspections and preventative maintenance
• Pumping system cleaning, repair and replacement,
• Metering system recalibration, repair and replacement,
0 Leachate collection system cleaning (e.g., jet rodding
for sediment buildup) and repairs,
• Manhole repairs (e.g., spalling or cracking) and cleaning
of sediment buildup,
• Drainage structure cleaning and repairs,
• Repair of erosion or seepage channels in the cap and
areas that may not drain properly,
0 Reseeding and refertilizing as necessary to maintain
vegetative cover on the cap,
• Mowing ae^Qeoessary to control deep rooted crops (e.g.,
trees) which could compromise cap integrity,
0 Groundwater monitoring well redevelopment, if necessary,
9 Access road maintenance. '
-------
-18-
•
All maintenance items will be performed on an as-needed basis as
evidenced by the monitoring programs. Repair and replacement work
would be performed in. a manner equal to the original design standards
and specifications.
PROTECTIVENESS
The remedy is protective of human health and the environment through
on-site containment of wastes. As a result, the site has been
isolated from the pathways of migration by which contaminated water
could impact human and environmental receptors. Since the site
is located in an area of groundwater discharge and the nearest
public groundwater supply well is located 1 mile upgradient, the
major potential threat is surface water degradation. As expressed
previously, the remedy has successfully prevented direct contact,
with the landfill waste and mitigated leachate migration into
adjacent surface waters. Thirty year monitoring in conjunction
with scheduled operation and maintenance will ensure the long
term effectiveness of the remedy.
CONSISTENCY WITH OTHER ENVIRONMENTAL LAWS
CERCLA, as amended by SARA, requires that completed remedial
actions comply with applicable and/or relevant and appropriate
requirements (ARARs) of federal laws and more stringent promulgated
state laws. ARARs are classified into three (3) groups: ambient
or chemical specific, location specific, and action specific
requirements. .
Ambient or chemical specific ARARs set health or risk-based concen-
tration limits in various environmental media for specific hazar-
dous substances, pollutants or contaminants. These ARARs, i.e.,
groundwater, surface water and air pollution control standards
will not be addressed in this ROD. They will be incorporated into
the Post-remedial Environmental Monitoring Program and utilized
to evaluate the need for any additional remedial actions related to
the site.
Action specific requirements control or restrict activities
related to the management of hazardous substances, pollutants or
contaminants. Examples include RCRA regulations for closure of
hazardous waste landfills and Clean Water Act pretreatment standards
for discharge to Publicly Owned Treatment Works (POTW's).
Location specific ARARs restrict activities depending on the
characteristics of a s^Lte or its immediate environment. Pertinent
action and locatioh*specific ARARs are provided in Table 2
of Appendix 2.
Although RCRA hazardous wastes were not disposed of or moved about
the site after November 19, 1980, the«Federal and State RCRA
requirements governing site closure are to be considered relevant
and appropriate under SARA.
-------
-19-
The BFI South Brunswick Landfill closure included the placement of
a clay cap over the fill material. The cap was designed to achieve
a permeability of 1 x 10~7 cm/sec and thereby provide long term
minimization of liquid percolation through the landfill. The cap
was also graded properly in order to promote drainage and minimize
erosion. During the construction phase the clay cover was compacted
to prevent future cap settling.
In accordance with RCRA capping requirements, the permeability of
the cap is less than or equal to the permeability (10~6 to 10~7
cm/sec) of the natural sub-soils present at the site, thereby
preventing infiltration which can lead to leachate mounding
within the landfill. Finally, in order to restrict post-closure
use of the property to prevent damage to the clay cover, a locked
gate has been placed at the landfill entrance and "No Trespassing"
warning signs have been posted approximately every 50 feet along
the landfill perimeter. Furthermore, EPA has determined that a
fence should be constructed along the site perimeter to restrict
access, reduce any nuisance threat and preserve the integrity
of the remedial action.
While the selected remedy complies with the closure performance »
requirements set forth in 40 CFR Part 264, Subpart G; it does not
meet the standards contained in the New Jersey Administrative .
Code, which is part of a duly authorized RCRA program. Neverthe-
less, EPA has decided to waive the State's capping requirements
since the selected remedy (clay cap, slurry wall and leachate
collection system) at this site is achieving a standard of
performance equivalent to that required by the State regulations.
Furthermore, given the equivalent protectiveness of the remedy,
it would be impractical to disturb the existing 68 acre cap in
order to meet State capping requirements.
In order to continuously evaluate the effectiveness of the remedial
action in containing the waste and, ultimately protecting human
health and the environment, a Post-remedial Environmental Monitoring
Program shall be implemented over a 30 year period. Post-closure
maintenance of the remedy is addressed in the Operations and
Maintenance Program for this site.
In addition to the clay cap, a lea.chate collection system was also
constructed as part of the remedial action. The function of this
system is to collect leachate within the landfill and pump it to
Stony Brook Regional Sewerage Authority for treatment. As a
result, the Clean Water Act pretreatment standards are also
considered relevant and appropriate under SARA.
In August, 1981 a treatability study of the BFI-South Brunswick
Landfill leachat£ was*conducted to determine if the leachate was
acceptable for treatment at the POTW. The leachate was found to
contain low levels of volatile organics, acid and base/neutral
compounds and heavy metals.
-------
-20-
The ieachate can be described as free flowing (non-obstructive),
non-corrosive (pH 7.50) liquid that would not result in fire
or explosion or raise POTW influent temperatures above 104°F.
The current rate of discharge is 20,000 gallons/day. Leachate is
discharged during off-hours so as not to interfere with the POTW's
operation. The current Ieachate discharged complies with the
Stony Brook Regional Sewerage Authority's requirements, is spill-
proof due to the spill prevention design of -the Ieachate collection
system, and is monitored and reported monthly to the New Jersey
Department of Environmental Protection.
Location-specific ARAR's are governed primarily by Executive
Order 11990, Protection of Wetlands. The remedial actions taken at
the site have eliminated the off-site migration of contaminated
leachage thereby preventing, any further destruction, loss, or
degradation of wetlands.
NJDEP will provide EPA with chemical/ambient specific ARARs upon *
evaluation of the initial sampling results from the post-remedial
monitoring program.
COST EFFECTIVENESS/PERMANENT SOLUTIONS/ALTERNATIVE TREATMENT
TECHNOLOGIES
The remedy was selected on the basis of its implementability and
proven effectiveness in landfill containment given the hydrogeology
of the site, size of the landfill and waste disposal practices.
The landfill accepted predominantly municipal waste.which was
comingled with hazardous waste. Since discrete areas of
hazardous waste disposal could not be adequately identified,
excavation, off-site disposal and/or treatment of contaminant
hot spots was not considered feasible. Excavation and disposal/
treatment of the entire 68 acre landfill was considered
impracticable and not cost-effective.
A reduction in the toxicity, mobility and volume of contaminants
is achieved by the remedy through treatment of collected Ieachate
at the Stony Brook Sewage Treatment plant. Analysis has shown
the quality of Ieachate discharging to the treatment plant improving
over time indicating a reduction of contamination within the
landfill.
*%* *
Given the limited scope of practical remedial alternatives for a
landfill the size and nature of BFI South Brunswick the containment
option selected and implemented represents the cost effective and
environmentally sound approach toward4site remediation..
-------
-21-
STATE ACCEPTANCE OF REMEDY
The NJDEP agrees that the on-site containment system in conjunction
with the 30 year post-remedial monitoring program will be protective
of human health,and the environment. Accordingly, NJDEP has concurred
with the remedy.
COMMUNITY RELATIONS
A public availability session was held at the South Brunswick
Township Hall on August 6, 1987. Concerned citizens were informed
of the remedial actions taken at the site and the proposed post
remedial monitoring plan. The public comment period which began
on that day closed on September 4, 1987. Upon request, the comment
period was extended until September 9, 1987. Concerns expressed by
the public are addressed in the Responsiveness Summary appended .
to this document (Appendix 5). Overall, the public and local
officials have expressed satisfaction with the selected remedy *
and the time-frame in which it was implemented.
FUTURE ACTIONS
Any future actions at the site are dependant upon the results of
the post remedial monitoring study. The study will address Federal
and State ambient and chemical specific ARARs which will be utilized
to evaluate the need for additional remediation.
-------
LIST OF APPENDICES
APPENDIX 1
GROUNDWATER QUALITY DATA FROM BYDROGEOLOGIC INVESTIGATION
(Table 1)
APPENDIX 2
SELECTED ACTION AND LOCATION SPECIFIC ARAR's
(Table 2)
APPENDIX 3
DATA FROM JUNE, 1980 EPA INVESTIGATION
APPENDIX 4
LEACHATE QUALITY AND VOLUMETRIC DISCHARGE DATA
APPENDIX 5
RESPONSIVENESS SUMMARY
-------
APPENDIX 1
GROUNDWATER QUALITY DATA FROM HYDROGEOLOGIC INVESTIGATION
(Table 1)
-------
TABLE 1
aiooND-wATBft QUALITY DATA
Ai«Mt 11, 1991
If eH
W-f
/•-19
»-ll
B-S
D-t5
B-10
B-17
• D-19
MP-1
j^
MP-2
MP-3
MP-4
MP-5
NJDBP
Chloride
* T-8
i f./
. 8.2
49.8
297
12.)
14.4
173
292
29.3
112
27.3
49.9
289
Stifle
^^flMflaaaawaaaaaaftafc
^^^^^^^•w^p^^^^rw
(*"*ateL.
129
1*9
179
449
2,299
1,990
209
lfS23
939
132
919
99
99
—
Dissolved
Solids
Total
149
199
199
319
1,329
94
39
919
•
.
.
••
Class GW-f •
Standard
Notest
'Total
*TnUl
_
volatile organic
nnn-vol«lll« MM*
•«!«•
-------
TABLE l, PAGE 2
aiOtnUMTATBR QOALTTT DATA
*s A^ sr "jar's?11 a a "w •&-»•'•. ...
«-• O.OOll *0.89 ».M <»,9MS <,.M| <,.,, ..
www" P.V
••» •••» •••» I.MI ..„ ,.„ M
•
-------
APPENDIX 2
SELECTED ACTION AND LOCATION SPECIFIC ARAR's
(Table 2)
-------
SELECTED ACTION-SPECIFIC ARAR's
TABLE 2
ACTIONS
CAPPING
264.22B(a)
REQUIREMENTS
Plaoenent of cap over waste
(e.g., clotting a landfill, or
closing a surface impoundment
or waste pile as a landfill, or
similar action) requires a cover
designated and constructed tot
0 Provide long-term Minimiza-
tion migration of liquids
through the capped areas
• Function with minimum
maintenance t
• Prorate drainage and minimize
erosion or abrasion of the
cover}
• Aooomodate settling and
subsidence so that the
cover's integrity is
maintained; and
• Have a permeability less than
or equal to the permeability
of any bottom liner system or
natural sub-soils present.
0 Restrict post-closure use of
property as necessary to
prevent damage to the cover.
RCRA hazardous waste placed at site
after November 19, 1980, or movement
of hazardous waste from one unit, area
of contamination, or location into
another unit or area of contamination
will make requirements applicable.
Capping without such movement will not
make requirements applicable, but
technical requirements are likely to
be relevant and appropriate.
CITATION
CFR 264.310(a)
(Landfills)
40 CFR 264.117(c)
-------
SELECTED ACTION-SPECIFIC ARAR's
TABLE 2 (continued)
ACTIONS
Closure with
Waste in Place
(Capping)
Operation and
Maintenance
(OSM)
Discharge to
REQUIREMENTS
Eliminate free liquids by
removal or solidification.
Post-Closure care to ensure
that site is maintained and
monitored*
Pollutants that pass-through
the POIW without treatment,
interfere with POIWt
operation, or contaminate
POIW sludge are prohibited.
Specific prohibitions preclude
the discharge of pollutants to
POTSs that:
0 Create a fire or explosion
hazard in the POIW;
0 Are corrosive (ph<5.0)j
0 Obstruct flow resulting
interference;
PREREQUISITES
Disposal of RCRA hazardous waste
(listed or characteristic) at site
after November 19* 1980, or move-
ment of hazardous waste from one
unit, area of contamination, or
location into another unit or area
of contamination. Not applicable
CITATION
40 CFR 264.29
to material undisturbed since
November 19, 1980.
40 CFR 264-1
40 CFR 403.5
-------
SELECTED ACTION-SPECIFIC ARAR's
TABLE 2 (continued)
ACTION
Discharge to
POIW (cont.)
REQUIREMENTS
• Are discharged at a flow
rate and/or concentration
that will result in inter-
ference} and
• Increase the temperature of •
wastewater entering the
treatment plant that would
result in interference, but
in no case raise the POTW
influent temperature above
104*C).
0 Discharge must comply with
local POIW pretreatnent
program, including.POTW-
specific pollutants, spill
preventation program require-
ments.
PREREQUISITES
CITATION
40 CFR403.5
and local POIW
regulations
-------
SELECTED LOCATION-SPECIFIC ARAR's
TABLE 2 (continued)
ACTIONS REQUIREMENTS PREREQUISITIES CITATION
Wetland Action to odniaia* the des- Wetland as defined by Executive Order Executive Order
truction, loss, or degradation 11990 Section 7. * 11990, Protection
of wetlands of Wetlands, (40
*» CFR 6, Appendix A)
*
-------
APPENDIX 3
Data From June, 1980 EPA Investigation
Content
Organics Results of Water Samples
Metals and Sediment Analysis
Comparison of Monitoring Well. Data
Comparison of Surface Water Data
Comparison of Sediment Analysis
Previous Well Data (6/20/76-
7/21/78)
Gl - G 2 Groundwater Data
Hi Sketch of Sampling Locations
II Review of Analytical Contractor
Results by the NEIC
4
-------
WEST COAST TECHNICAL SERVJCE INC INDUSTRIAL CATEGORY.
3AMPLE ID B0101
SAMPLE ID B0101
.AB ID 19601A1
MTE EXTRACTED
)ATE INJECTED
;TD ID OFTPP1066
lONC FACTOR
PS Iof39
6/15/80
7/7/80
PHENOL244
1000
LAB ID 19601B1
DATE EXTRACTED
DATE INJECTED
STD ID OFTPP1070
CONC FACTOR
6/14/80
7/11/80
BNSTD272
1000
I
eld Compounds
1A
2A
'.A
LA
1A
•A
A
A
A
A
A
2 , L . 6-trichlorophenol
p-chloro-m-cresol
2-chlorophenol
2.4-dichlorophenol
2,^-dimethvlphenol
2-nitrophenol
i-nitrophenol
2,4-dinitrophenol
4,6-dinitro-o-cresol
pentachlorophenol
phenol
NO
ND
ND
ND
NO
NO
NO
ND
ND
NO
*
se/Veutral Compounds
acenaphthene
benzidine
1 , 2. £-triehlorobenzene
hexachlorobenzene
hexaehloroethane
bis(2-chloroethvl)ethtr
2-chloronapthalene
1 , 2-dichlorobenzene
1.3-dichlorobenzenc
1 ,^-dichlorobenzene
3.3'-dichlorobenzidine -
2.^1-dinitrotolucnc
2.6-dinitrotoluene
1 . 2-dipheny Ihydrazinc
(as azobcnzene)
fluoranthene
ND
ND
ND
ND
ND
ND
ND
NO
ND
NO
ND*
NO
NO
ND
ND
Base/Neutral Compounds ug/1
41B
42B
43B
52B
53B
54B
55B
56B
61 B
62B
63B
66B
67B
68B
69B
70S
71 B
72B
73B
74B
75B
76B
77B
78B
79B
808
81B
82B
83B
4-bromoohenvl phenvl ether
bis(2-chlorotsopropvl) ether
bis (2-chloroethoxv) methane
hexachlorobutadiene
hexachlorocvelopentadiene
isophorone
naphthalene
nitrobenzene
N-nitrosodimethvlamine
N-nitrosodiphenvlamine
N-nitrotodi-n-propvlamine
bis (2-ethvlhexvl) phthalate
butyl benzyl phthalate
di-n-butyl phthalate
di-n-ocTvl phthalate
diethvl phthalate
dimethyl phthalate
benzo(a) anthracene
benzo(a)pvrene
3.4-benzofluoranthene
benzo( k ) fluoranthene
chrvsene
acsnaphiiiwlene
d. ..!.•.!.. ...1?
benzo( £hi Jpervlene
fluorene
phenanthrene
dibe*zo( a. h) anthracene
indeno(1.2.3-cd)pvrene
ND
ND
ND
ND
ND
ND
*
*
ND
NO
NO
ND
NO
*
NO
NO
NO
NO
NO
NO
NO
ND
Np
ND
ND
ND
MO
NO
MO
pvrene
T .
-------
W6ST COAST TECHNICAL S€RVIC6 INC.
BONN *
INDUSTRIAL CATEGORY
JPLE ID
ID 19601V1
DATE INJECTED
S7D ID DFTPP1052
CONC. FACTOR
Volatiles
2V acrolein
3V acrvlonitrile
4£2.fiL?i_
6/19/80
T9600V7
£V
benzene
6V carbon tetrachloride
TV chlorobenzene
10V 1.2-diehloroethane
11V 1.1.1-trichloreethane
13V 1.1-dichloroethane
1.1.2-trlehloroethane
1,1.2.2-tetrachlorbethane
16V chloroethane
19V 2-chloroethvlvinvl ether
23V chloroform
29V 1,1-dichloroethvlene
30V 1.2-trans-dichloroethvlene
32V 1.2-dichlorooropane
53V 1,3-diehlorcoroovlene .
?8V ethvlbenzene
.LM methvlene chloride
•5V methvl chloride
•6y methvl bromide
.7V bromoform
•8V dichlorobromomethane
7V
dichlorodifluoromethanc
IV chlorodibromomethane
5V tetraehlorcethvlent!
5V toluene
ug/1
ND
ND
23
ND
ND
JSL
.£!
JJP_
NO
ND
105
48
59
ND
NO
ND
30
NO
NO
..NIL.
Jin.
MO
NO
NO
MO
SAMPLE ID B0101
LAB ID TRACE 1538
DATE EXTRACTED . 6/14/80
DATE INJECTED 6/20/80
STD ID TRACE 1532
CONC. FACTOR 100
Pesticides
89P aldriTi
90P dieldrin
91P chlordane
92P 4,4 '-DDT
93P 4. 4 '-DDE
ug/1
ND
ND
ND
ND
NO
94P 4,r-DDD NO
95P alaha-endosulfan
96P beta-endosulfan
97P endosulfan sulfate
98P endrin
99P endrin aldehyde
100P heptachlor
101P heotachlor epoxide
102P aloha-BHC
103P beta-BHC
104P gamma-BHC
105P delta-BHC
106P PCB-12^2
IOTP PCB-1254
108P PCB-1221
109P PCB-1232
HOP PCB-1248
HIP PCB-1260
112P PCB-1016
113P toxaphene
NO.
NO
ND
ND
NO
NO
NO
NO
1.06
NO
NO
ND
NO
ND
ND
ND
NO
NO
NO
* • Less than 10 ug/1
:»x strides less than 5 ug/1)
ND « Not detected
-------
W65T COAST TECHNICAL S€RV1CE INC
ORGANICS ANALYSIS DATA SHEET - Page 3
^
^_ ^ Sample .Nunoer
\'o: 10 PS_3o 3^ BOiOi
f*~~ A. SURROGATE S?I. 3/N '' «4 • 103 ! 61
2-?luorobi5henvl i 3/tf I 22 | 103 | 21
1 1 1 I
i
CAS
8. TENTATIVELY I2£NTI?IE3 CCWPCUNOS
2 Maximum Score Attalnea
1 i COMPOUND NAME FRACTION Mass Matching Routine: FIT
soecifv;
L
CHLOROOIFLUORCMETHANE VOA*32 947
J2. 1,T -OX YBYS ETHANE VOAI147 980
13. i '
4.
5. !
6. i
7. i
!s.
ig. i
10. !
i' i
• • •
'12.
Il3,
'•14. !
'15. '
'15. :
TRIMETHOXYMETHANE VOW 195 869
UNKNOWN VOAI359 NO GOOD FITS
i UNKNOWN VOAtf398 j NO GOOD FITS
i UNKNOWN ACIDH341J NO GOOD FITS •
i UNKNOWN ACIOJ365J NO GOOD FITS
i N.N-OIMETHYLFORAmOE AC 1 0*42 961
3,3.5-THIMETHYL CYCLO-I
i . HEXANONE; BrU9 • 973
1 A.Fl'JORO-l.r-BIPHENY'j ACID*129t 991
! N.N-OWETHYLFORMAMIDE ' 3#93 894
UNKNOWN . 8*107 W GOOD FITS
UNKNOWN^ * Bfl70 NO GOOD FITS
j 3.5.5-TRIMETHYL-2- - i j
i CYCLCHEXEN-1-ON6 3f197 i 906
18.:
-------
W€ST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY.
SAMPLE ID 30102 \jj£LL 2
^ ID 19601A2 03 #6^39
DATE EXTRACTED 6/15/80
"DATS INTSCTED 7/7/80
STD ID OF7PP1066 PHE?lOL24A
' CCNC r ACTC3 1000
Acid Compounds •• u
21 A 2.1.6-trichlorooher.ol
22A o-chloro-m-cresol
2£A 2-chleroohenol
31 A 2.i-
-------
/
,,<£^ W6ST COAST TECHNICAL S€RVH
'' .AMPLS ID 30102 WEIL *2
LAS ID 19601V2 95 5*0^3^
DATS INTECTED 5/20/80
STD ID OFTPP1052 1960CV7 - .
Volatiles
2V acrslein
JV tcrvlcnitrilt
£V benzene
6V carbon tetrachloride
TV chlcrsbenzene
1CV 1.2-dichlorcethane
1 IV 1,1. 1-trichlorsethane
13V 1 . l-dichlcrcethane
UV 1.1. 2-trichlcroethane
15V 1.1.2.2-tetrachloreethane
\ 16V chlorsethane
. •
mxx*^et£t$^i(£(*x2x;tt£tfxxxxx
19V 2-chlorsethvlvinvl ether
23V chlcreforsi
29V l.l-dichlorsethvler.e
ug/l
NO
NO
42
NO
17
NO
NO
NO
NO
NO
NO
XXX
NO
NO
NO
30V 1.2-trans-dichlcrsethvlene 48
32V 1.2-dichlorsorroane
33V 1 . 3-dichloroorsovlene
:SV ethvlbenzene
i-V methviene chlor.de
&1 methvl chlor.de
iSV rrethvl brswde
LT1 brsireform
iSV dicr.lcrobrcfnor.etnane
^?V trlchlcrsfluorcsetnane
50V dicMsrsdi.'lucrsrretrvane- .
51V chlarscibrsmonethane
NO
NO
58
22
NO
NO
NO
NO
NO
NO
NO
35V tetrachlsrcethvlene nn
55V tciuere
19*3
5T7 tTtshlorsethviene •
SAMPLE ID B0102-
LA3 ID TRACE #541
DATE EXTRACTED 6/14/80
DATE INJECTED 6/20/80
STD ID TRACE 4532
CONC. FACTOR 100
Pesticides
89? aldrin
90? dieidrtn
91? ehlordane
92? L.L '-DDT
93? 4.i'-DDE
ug/l
0.120**
ND
NO
NO
NO
94? 4.-i'-DDD NO
95? aloha-endssulfan
96? beta-endssulfan
97? endosul'an sulfate
98? endrin
99? er.drin aldehvde
100? heotachlor
NO
NO »
NO
NO
NO
Q.7Q**
101? heotachler eooxide n .?•»*•»
102? aloha-BHC
NC
103? beta«BHC NO
104? gamma-3KC
105? delta-3HC
NO
O lfi*w
106? PC3-1242 in
107? PCS-1254
103? PCS-1221
109? PCS-1232
MH
"in
•in
110? PC3-1243 MO
111P PC3-1260
112P PC3-1016
113? toxaohene
MO
NO
NO
* • Less than 10 ug/l
{pesticides less than 5 ug/l)
MD « ^c: detected
•*'» Mot csn/irned by CCMS
-------
S3ga W6ST COAST TECHNICAL S6RV1C6 INC
CRGANICS ANALYSIS DATA SHEET - Page 3
No:
10
sanie Numoer
A. SURROGATE 5?i:<2 RESULTS
l-C*.lere-2-3rs»ecrc«ar.«
VOA
47.5
50.0
1 95
j COMPOUND
i
i
• Fraction
1 i i Surrooetes only;
i Conc.(uo/l)
i splice
i Added (uo/1)
i Bcns«r.a - d6
•: VOA
1 51.7
! 50.0
s
Recover/
103
Toiu«n« - d8
VOA
70.7
50.0 1 141
2-?luoroah«nol
ACID
NO
108
I
Phenol - d5
ACID
MO
105
Ni±reber.2er.c - d5
B/N
51
103.3
50
! 2-riucrobisher.vl
! 3/N '
114
; 102.6 |
112
3. TNTATIVELY IDENTIFIED COMPOUNDS
9 CAS 4
CCMPOUN: :JA«E
FRACTION
S Maximum Score Attained
Mass Matching Routine: FIT
I'soecify
ii. i
t.
b. !'
2-PRCPANONE
2-PROPANOL
OIME7HOXYV-7HANE
VOAI84
VOA^IOO
VOA#115
!4. •' 1,r-OXY5'S£7HANE { YOAW7
:s. :
2-3UTANC.-M
:6. j i 2-SUTANOL
7. :
8. !
19.
.10. '
•11..:
12. '
13. :
A:
!•• . '
-15.
;* *
• • • .
13. :
j 2-PE.NTA.NONr:
voAfiei
988
979
993
994 |
970
VOA#176 i 961
VOA*245
955 i
i l,3-OICHs.'-r.:-2-PSCPA,NQNE VCA#272) 852
• i
4-a£THYL-i----.%TANONE
VOA^306
966 i
! ETHYL3E.NZE i 2-HEPTANQNE VOAf425 • 997/944
; UNKNOWN
i UNKNOWN
i UNKNOWN
UNKNOWN •"*« "
; UNKNOWN
i UNKNOWN
. JNOCWN
i
UNKNOWN
ACID-62
ACID»S6
NO GOOD FITS
NO GOOD FITS
ACIDI107I NO GOOD FITS
ACIC»U2; NO GOOD FITS
ACIDf 1571 NO GOOD FITS
AC I Of 194) .NO GOOD FITS i
i
ACID»221P -JO GCCO FITS
ACID-233! NO SOOO FITS !
: ' -
-------
WEST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY.
SAMPLE ID 80103
LAB ID 1960183
DATE EXTRACTED 6/1 A/80
DATE INJECTED 7/11/80
STD ID DF7PP1071D BNSTD273
SAMPLE ID 30103 LUfcU-
LAB ID 19601A3 P5 7 C
DATE EXTRACTED 5/15/80
DATE INJECTED 7/7/80
STD ID OFTPP1066 PHSMOL244
C2NC FACTOR 1000
Acid Ccmoounds
21 A 2.i.6-trichloroohenol
22.1. o-chlsrs-rr.-crssc!
2L.\ 2-chlcroohenoi
31 A 2.1-dichlsr3ohenol
3iA 2.1-dimethvlohenol
57A 2-nitroohenol
53A i-nitroohenol
59A 2.1-diP.itrcohenol
cCA L . o-dinitro-c-crssoi
5iA oentachlsroohenol
\ 65A ohenol
>
Base/Neutral Comoeunds
13 acer.aohthene
53 benzidir.e
33 1.2.^-trichlerobenzene
93 hexachlorsbenzene
123 hexachlorcethane
1S3 bis<2-chlore«thvl.»eih«r
2CB 2-chloronaothaUnc
253 1 . 2-dichlor3benzene
263 1.3-dichlsrsbenzene
273 l.i-dichicrobenzene
253 3.3'-dicr.lor3benzidine
353 2.i-dinitrotoluene
363 2.3-cinitrst3lu«ne ***• "*
373 l,2-di?henylhydrazine
353 fluct-antr.sne
,103 i-chicrsorenvi -henv; tth.
3
**3=t
ug/l
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
MO
MO
MO
MO
erND
CONC FACTOR
1000
Base/Neutral Compounds - ug/l
A1B £-bromoohenvl ohenvl ether NO
£23 Msf2-chloroisooreov!) ether NO
£33 bis (2-chloroethoxv) methane NO
523 hexachlorcbutadlene NO^
53B hexachlorscvclooentadiene NO
543 isoohorone NO
553 naphthalene NO'
563 nitrobenzene NO
513 N-nitroscdirsethvlamine NOJ
623 N-nitrosodio'nenvlanine NO
633 N-nitrosodi-n-orcovlareine NO
663 bis (2-ethvlhexvl) ohthalate NO
678 butvl benzvl ohthalate
683 di-n-butvl ohthalate
698 dt-n-octvl ohthalate
708 diethvl ohthalate
713 dimethvl ohthalate
728 benzo(a) anthracene
738
733
benzoia)ovrene
7£B 3.^-benzsfluoranthene
753 benzo(k)fluoranthene
763 chrvsene
773 acenaohthvlene
anthracene
798 benzo(ghi)oervlene
SOB fluorenc
913 ohenanthrene
323 dlbenzo(a.h)anthracene
33B tndeno<1.2.3-cd)ovrene
Si3 *ovrene
1298 2.3.7.3-tetrachlorodibenso-
o-dioxin
NO
NO
11
NO
NO
MIL
MO
MO
Mf>
JiL
NO
MQ
MD
MQ
NO
-------
W6ST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
*i..f»..r - 3C103 WELL «
^T- Z.MJSrTID 6/20/80
=7D ID 3FTPP1053 19600V9
Velatiles
2V acrolein ~
jV acrvlcni:rtle
£V benzene
5V carbon tetrachloride
TV chlorobenzer.e
10V 1 . 2-dichloroethar.e
11V 1,1.1-trichlorcethap.e
13V 1.1-dichlcroethar.e
\L\T 1,1.2-trichiersethane
15V 1.1.2.2-tetrach:oroethane
flfctf chlarcethane
^••T •
T7 /X X Xtt !«CttCZ JectJSJJl X S T.( !£ X X*X XCeXX X X X ?
19V 2-chloroethvlvtnvl ether
23V chlorofcrm
29V 1 . 1-dichloroethvler.e
3CV 1.2-trans-dichlcrcethvlene
32V l.2-dichlorsors«ane
33V 1.3-dichlors9roovle«e
3SV etr.vlbenzer.e
LL'I r.ethvlene chloride
i3V methvl chloride
.ioV rsethvl bromide
CFI brarsoforn
• £SV dichlorobrsr.crr.ethane
i9V tnchlcroflucrsrr.ethane
5CV dichlorodiflucrer.ethane
^aiV chlerceibrsr.ametharttev* •*
^P^ tetrachloreetrtvler.e
S6V tsiuene
57V tr-.shlsrcetr.vler.e
39
ug/l
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
*
(XXX
NO
NO
NO
NO
MO
MO
MO
10?
NO
NO
NO
MO
MO
17
MO
MO
MO
'10
SAMPLE ID 30103
LAB ID TRACE «542
DATE EXTRACTED 6/14/30
DATE INJECTED 6/20/80
CTf\ 1T\ TDflrC •C^'9
siu ID ! KAtt *3JZ
CCNC. FACTOR TOO
Pesticides
S9P aldrin
SOP dieldrin
91P chlordane
92? ^.i'-DDT
93? i.^'-DDE
9i? ^.^-DDD
95? aloha-endcsulfan
96? beta-endcsulfan
97? endcsul/an sul/are
98? endrin
99P endrin aldehvde
1 AAB WA^MA.^IA^
lOCr he^tachlor
101? heotachlor eoexide
102? aloha-3HC
103? beta-3HC
lO^P samma-3HC
105? del:a-3HC
IC6? PC 3- 12^2
107? PC3-i25i
108? PC3-1221
109P PC3-1232
HOP" PC 3- 12^3
111? PC3-1260
112? PC3-1015
113? toxaohene
•' m Less than 10 ug/l
(pesticides less than 5 ug/l)
ND » Met detected
** « Mit confirmed by GCMS
"ue/l
NO
•;0
NO
NO
MO
NO
NO
NO
NO*
NO
NO
- NO
MO
NO
NO
NO
MO
NO
MO
MO
MO
MO '
vn
vn
Nn
A
S6V v.nvl chloride
-------
£gj W€5T COAST TECHNICAL S6RV1C6 INC
ORGAN!CS AiNALYSIS DATA SHEET - Page 3
CC Sesort No:
1 W ' fc^fc« f fj ' ^J |
{ Sample .Nurraer
i 30103
A.
57i.\£ fCtSu
CCMPCUNO
• Benzene - d6
Fraction
VGA
1
1 Conc.(uo/1)
j 52.0
Surrooates only) i
5pi*
i
1
i
:
FRACTION
VOAf30
VOAI71
VOAI85
VOA#195
ACIO^lOO
'
.
2 Maximum Score Attained
Mass Matching Routine: FIT
f soeclfy
958
950
957 |
921 |
932
•
j
!
•
•i
j !
i
I • 1
.
•18. '•
-------
WEST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
30104
CAMPLE ID
ID 19601A6
/D of
DATS EXTRACTED.
DATE INJEOTSD_
STD ID
6/15/30
7/7/80 .
OF7PP1067 PHEN 2*5
CCNC FACTOR "1000
Acid Compounds
21A 2,^.6-trichloroohenol
22A p-chlcro-m-cresol
2-chlorophenol
31A 2.£-dlchlorcphenol
2.£-dlr.ethvlphencl
57A 2-nitTCPher.el
5eA £-nitrop'nenol
59A 2.1-dinttTcohenol
60A £.5-dinitro-o-cresol
pentaehlorophenol
phenol
Base/Neutral Compounds
13
acenaphthene
53 ber.zldlne
S3
1.2.i-tr*.ch!crcbenzene
93 hexachlers'oenzene
123 hexachlcrcethane
153 bisf2-chloroethvl)ether
203 2-chlcranapthaUnt
253 1.2-dtchlorsbengene
253 :.3-dier.Ior3benzer.e
273^ 1_._^ «
-------
VV6S7 COAST TECHNICAL S6RVICS INC INDUSTRIAL CATEGORY
»!£ ID 3C104
IA3 ID 19601V17
DATS INJECTED
STD ID DFTPP1054
CCNC. FACTOR
Volatile*
o<; //
6/21/30
19601715
2V
3V
TV
acralein
acrvc
IV benzene
6V carbon tetrachlcrice
chlsrober.rer.e
IOV 1.2-diehlsrsethar.e
1IV 1.1.1-trtchlcrsethane
13V 1.l-dichlorsethane
UV 1.1.2-trich:orsetr.ar.e
15V 1.1.2.2-tetrachlercethar.e
16V chloreethane
17V bis(ehlororr.ethvl) ether
19V 2-chloroethvlvinvl ether
23V chloroform
29V 1.1-dichlorcethvler.e
32V 1.2-dtchIorst»rcoane
33V l.3-dichlc«
38V gtr.vlbensene
UV aethvlene chloride
I5V methvl ehleridt
iSV ffethvl brcr.idg
IT^f brsnefcrm
-3V d:chlor;br;r.or!»ethaRe
i9V trichlcrofluorsff.ethane
5 1 V cr. Icrsc : b rrr.err.et har.e
S5V
'* *
retrachlarretnvl-r.e
55y toluene
3^«' ?r:;hlor;etr.v'.ene
3SV vinvi chicride
ug/1
NO
NO
NO
NO
NO
NO
NO
NO
ND
NO
ND
ND
ND
ND
ND
30V 1.2-trans-diehlsrsethvlene NO
HP
HO
NO
QQ
MP
MO
MO
—HO
MO
...MO
NO
ND
MO.
NO
SAMPLE ID 30104
LA3 ID TRACE -544
DATE
DATE
EXTRACTED 6/14/80
INJECTED 6/20/80
STD ID TRACE »542
CCNC.
Pestic
S9P
SCP
91?
92?
93?
94?
95?
96?
97?
98? .
99?
100?
101?
102?
103?
10£P
105?
106?
107?
IC0P
109?
HOP
ill? .
112?
113?
FACTOR 100
ides
aldrin
dieidr-.n
chlcrdane
i.r-DDT
£.r-DDE
4.£'-DDD
aloha-endosul/an
beta-*ndcsulfan
endcsulfar. sulfate
endrin
en drift aidehvde
heotachlor
heotachlor eooxide
al?ha-BHC
be:a-3KC
?amma-3HC
delta-3HC
PC3-1212
PC3-125^
PC3-1221
PC3-1232
PC3-l2iS
PC3-1260
PC3-1016
toxaohene
ug/1
NO
NO
MO
NO
NO
NO
NO
NO
NO-
NO
NO
NO
NO
NO
MO
NO
NO
MO
MO
MO
NO
NO
NO
MO
NO
* • Less than 10 ug/1
(pesticides less than 5 ug/1)
SD «• Not detected
•••• Not confirmed by GCMS
4_1 1
-------
sort Mo:
10
WEST COAST TECHNICAL SERVICE INC
ORGANIC* ANALYSIS 2ATA SHEET - Page 3
Sampie Numoer
30104
- A.. SURROGATE SPIXE RESULTS
1
i - 1
i COMPOUND !• Fraction
1
! Cone.
1 (Surrooaies only) i
1 Spue i -s
(uo/1) ' Added (uc/1) ! Recovery
! Ser.ter.e - d5 ! VOA
i
! Tolusr.e - d8
i
i VOA
1 2-?iuorocher.ol ' i ACID
i Phar.cl - d5
• ACID
i Nitrcber.ser.e - d5 • 3/N
1 2-?luerobi9her.vl ' 3/N
i
1
1 52
! 47
1 51
! 33
i 80
j 66
! 38
1
! 50 ! 104
i . 50 1 94
1 50 1 102
1 108 1 31
i 105 1 76
1 103 J 64
i 103 i 86
i !
•
3. TENTATIVELY
ICENTI?
I ED COMPOUNDS '
i i
| | CAS,
j
COMPOUND NAME j
FRACTION
1 5 Maximum Score Azialneo
Mass Matching Routine: FIT
1 'ToecTfv]
!i !
•10. !
2-PROPANONE
IVOAf87
970
i2. j ! TRIMETHOXYMETHANE ;VOA#195 j 925
i'3. 1
'4. !
5. i
!. -: 1
1 i 1
i : • i
:e. .! 1 i 1
17. i
! { i i
*. i I i !
19. !
1 i 1 i
!rr i
I13..I
.13. :
no
•
-------
WEST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY.
SAMPLE ID B0105
SAMPLE ID 80105
LAB ID 19601A7 K ~\*\ t
DATS EXTRACTED 5/15/30
DATS INJECTED 7/7/80
STD ID OFTPP1067 PHEN 245
CCNC FACTOR 10GO
Acid Compounds
21A 2.£.6-trtchlorophenol
22A o-chlorc-rr.-cresol
2£A 2-chlorophenol
31A 2.i-dichlorophenol
3£A 2.£-di:r.ethv!rhenol
37A 2-nttrophenol
5SA i-nitrop'r.enol
5?A 2,£-dinitrophenol
5CA £.6-dini:ro-2-cresol
6£A pentachlerep'nenol
65A phenol
3ase/N'eutral Compounds
13 acenaphthene
53* benzidine
S3 1.2.£-trichlcr:ber.zene
53 hexachlcrsbenzene
123 hexachleroethane
153 bif'2-chlcrsethvUether
2C3 2-chlcrsnapthalene
253 1 . 2-dichlorobenzer.e
253 1.3-dichlcrabenzene
273 l.i-dichlerobenzene
2S3 3.3*-iichiorsbenzidine
353 2.£-
-------
_ WEST COAST TECHNICAL SERVICE INC. INDUSTRIAL CATEGORY.
' «AMPLE ID 80105 WELL *3
VB ID 1960177 PS /«/
DATS INJECTED " 5/20/80
STD ID DFTPP1053 "196COV4 -
Voiatiles
2V acrslein
3V acrvlonitrile
£V benzene
6V carbon tetrachloride
TV chlarcbenzene
1CV 1.2-dichlorcethane
1 IV 1.1. l-rrichlorsethar.e
13V 1 . 1-dichlorsethane
. UV 1.1. 2-trlchlcrcethar.e
jfU l.l,2.2-:etrachloroethar.«
^eW chloroethane
X2KXX xawxas if«a»« jtx:i:cx:«cKcs( x xx
19V 2-c'nleroethvlvinvl ether
23V chloroform
29V 1 . 1-dichlorcethvlene
30V 1 . 2-trans-dich!orsethv:ene
32V 1.2-dichloroorooane
33V 1.3-dichicro3rosvlene
3SV ethvlbenzene
£iV nethvlene chloride
£5V netr.vl chloride
i6v r.ethvl bronide
i7^/ brsRiofsrr.
1SV dichlorcbrcrr.rr.etha.-.e
iSV trichloror'luorsrnethane
fCV cithisrrdi.lucrstrethApfi' 4
^B chlrr5dibr5r.cr.etr.ar.*
3^V ••»»•/•'•' ^*^*r^ v' ^***
^» J * »t*««3W*4*wfc«C««*V,C««V
"oV *^:"*-»*
vWV *«s
MO
MO
Mn
»tn
vn
NO
NO
MO
NO
NO
NO
SAMPLE ID B0105
LAB ID TRACE *549
DATE EXTRACTED 6/14/80
DATE INJECTED 6/20/80
STD ID TRACE ?532
CONC. FACTOR 100
Pesticides
89? aldrtn
90? dieldrin
91? chlordane
92? £.r-DDT
93? £.r-DDE
ug/1
; NO
NO
NO
NO
NO
9£P 4,4'-DDD NO
95? aloha-endcsulfan
96? beta-endosulfan
97? endcsulfan sulfat*
98? endrin
99? endrin aldehvde
IOC? heotachlor
101? heotachibr eooxide
102? aloha-3HC
103? beta-3HC
10£? aamma-SKC
105? delta-3HC
1C6? PCS-12i2
107? PC3-125^
108? PC3-1221
109?- PC3-1232
11CP PC3-12iS
111? - PC3-1260
112? PC3-1015
113? texaohene
NO
NO.
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
MO
NO
NO
NO
* • Less than 10 ug/1
(pesticides less than 5 ug"/l)
N'D • Nojt detected
*•"• Nlot confirmed by CCMS
-------
s No:
WEST COAST TECHNICAL SERVICE INC
CRGANICS ANALYSIS 3A'A SHEET - Page 3
-ft
Sample .Nu
30105
A. SURROGATE SPIKE RESULTS
(Surrooaiaspn1v]
i CCMPCUNO
I |
! Fraction i
Conc.(ua/1)
i Spue
i Added (ua/1)
V I
"* " 1
Recovery i
- d6
VOA
53
50.0
105
;
! sn n
1 *U.U
; sn n
i 9U .U
! inn
I 1 UU
Toluene - d8
J VOA
56
50.0
j 2-Fl-zcresher.el
ACID
82
108
I 76
Phenol - dS
ACID
78
105
I 74
; Mi-ircber.zer.e - d5
i 2-?lucrcbiaher.vl
i
i
i 3/V 1 71 •
i 3/N I 86
i •• 1
1 103
! 103
1
69 |
84
1
I
9. T-NTAT/ELY ISEriTIFIES
1
CAS
il. i
h.
3.
4. i
•5. :
6. i
.7. '
8. 1
•9. :
110. J
•« « i
• • . :
12. :
!ii
• ^ •
114.
«i : :
. • * • '
# CCM.POUNO NAME
il.T-OXYSIS ETHANE
JTRIMETHOXYMETHANE
IM-METHYLENE BIS(OXY)-
il-ETrfOXY-BUf^t^'-
iUNICIOUN
iCHLORCBEMZEaE '
jUMCtCM
iUNXNOUN
IUNK.NOUN
i
*•-!_'••
.:
FRACTION
0
VOA#145
VOA4195
Vnfl^7«5
VOA«20
ACIO¥339
B/Nf60
3/N481
B/NI187
B/NI468
3 Maximum Score Attained
Mass Matching Routine: FIT
i soecifvr
913
944
Q8?
961
NO GOOD FITS
964
NO SOCO FITS
NO 6000 FITS |
NO GOOD FITS )
!
1
•
. i
'17. >
-------
W6ST COAST TSCHNICAL S6RV1CE INC. INDUSTRIAL CATEGORY.
SAMPLE ID B0106
SAMPLE ID B0106
A
LAB ID I960! AS tt-lL
VTE EXTRACTED 6/15/SO
DATE INJECTED 7/7/80
STD ID OFTPP1067 PHEM 245 -
CONC FACTOR 1COO
i
Acid Compounds .
21A 2,£.5-trichlorcohenol
22A o-chloro-m-cresci
2£A 2-chlcroohenol
31A 2.^-dichioroohenol
3£A 2.^-dirr.ethvlohencl
57 A 2-nitrooher.ol
5SA i-nitroohenel
59A 2.£-dir.itroohencl
5CA £.5-dinitro-c-cresel
. o£A oer.tachloreoher.ol
*H ohenol
9
Base/Neutral Compounds
13 acenaohthene
53 benz-dine
S3 l.2.£-:richlorabenzer.e
93 hexachlorcbenzer.e
123 hexachler?ethane
153 bis'2-chlcraethv:)ether
203 2-chlcronaoth*Une
253 1.2-dichlorob«nzer>.e
263 1.3-dichlcrobenzene
273 l.i-dichlorobenzene
253 3.3f-dichlorobenztdir.e
353 2.^-dinitrotoluene
^63 2.5-dinitratoluene «^ ' ^
^pB 1.2-diohenyihycrazine
393 flucranther.e
iC3 i-ch'.croohenvl oher.vl *th
a* .jfi
ug/l
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
154
NO
NO
NO
NO
NO
NO
NO
*
•
NO
"NO
NO
NP
NO
NO
erNO
LAB ID 19601B9
DATE EXTRACTED 5/14/80
DATS INJSCT3D 7/13/80
STD ID OFTPP1073 BNSTD 275
CONC FACTOR 1000
Base/Neutral Compounds u
£13 £-brorr.oohenvl ohenvl ether
£23 bis(2-chloroisooroovl) ether
£33 bis (2-chloroethexv) methane
523 hexachlorabutadiene
533 hexachlorocvclooentadiene
5£3 isoohorone
553 naohthalene
563 nitrobenzene
613 N-nitrosodlir.ethvlamine
623 N-nitrosodiohenvlamine
633 N-nitrosodt-n-oroovlamir.e
663 bis (2-ethvlhexvl) ohthalate
673 butvl benzvl ohthalate
68B di-n-butvl ohthalate
69 B di-n-octvl ohthalate
706 diethvl ohthalate
713 dimethvl ohthalate
723 benzoia; anthracene
733 benzoi a )ovrene
7i3 3,i-benzor"luaranthene
753 benzo(k)P.uoranthene
763- chrvsene
773 acenaohthv'.ene
78B anthracene
793 benz»(shi)oervlene
SOB Huorene
9 * 4 * '
323 dibenzo« a. h) anthracene
333 ind«no''1.2.3-cd»ovrene
:L3 ^pvrsr.e
1293 2.3.7,a-ietrachlor5Cibenzo-
g/1
NO
NO
NO
NO
NO
11
NO
NO
NO
NO
NO
NO
NO
*
NO
167
*
NO
NO
NO
NO.
NO
MO
NO
NO
NO
MD
Nn
-------
W6ST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
DATE INJECTED 6/20/80
STD ID DFTPP1053 15600V4
CCNC. FACTOR
Volatile*
2V acrolein
3V acrvlcr.itrl!e
LV benzene
6V carbon tetrachlgrtde
TV chlorabenzene
10V 1.2-c:ch:grsethar.e
I1V 1.1.1-trtshlorcethant
13V l.l»dleh!erse:hane
UV 1.1.2-trtchIgrgethar.e
I5V 1.1.2.2-se;rachlcrge;har.e
16V chlgrgethane
32V 1.2-dichlorg3rg?ane
33V l. 3-dlehlgrgorg9vt.er.e
51
55V
ScV
-9V •. r: = h I s r; fl u g r c T.e t h a n e
50V dichlgrgdifluory
tgluer.e
ug/1
NO
NO
81
ND
102
ND
ND
ND
ND
ND
58
19V 2-chlorstthvlvlr.vl ether ND
23V chloroform NO
29V 1. 1-dlchlorgethvlene NO.,
30V 1.2-tTans-dichlcrgethvlene 4A
NO
MO
160
LL'J
l&t
LBV
LTV
rr.etr.vlene chloride
r.ethvl chlsrtd«
s»e:hvl brerside
brsr.cfsrrn
147
NO
ND
ND
MP
SAMPLE ID 30106
LA3 ID TRACE #563 &S69
DATE EXTRACTED 6/14/80
DATS INJECTED 6/24/80
STD ID TRACE $571
CONC. FACTOR 100
Pesticides
89P aldrin
90? dieldrin
91? chlordane
92? £.r-DDT
93? ^.i'-DDE
9£? *..i'-DDD
95? aloha-endgsulfar.
96? beta-endosulfan
97? endosulfan sulfate
98? er.drin
99? endrin aldehvde
100P hestachlor
101? hestachlor eocxide
102P alt>ha-3HC
103P b«:a-3HC
ug/1
NO
NO
NO
NO
NO
NO
NO
NO
NO*
NO
NO
NO
NO
NO
NO
10*? aarnma-SHC **0.30
105? dei:a-3HC
1C6? PC3-1212
107P PC 3- 125£
NO
NO
ND
108P PC3-122: N5
109? PC3-1232
HOP PC3-l2i3
111? PC3-1260
112? PC3-1016
H3P toxaohene
NO
NO
vn
NO
NO
* • Less than 10 ug/l
(pesticides less than 5 ug/1)
ND » Nor detected
»" « >fct cgn/trned bv CCMS
56V v.r.vl ;h;gr:dg
17
A-!7
-------
EJffiS W€ST COAST TECHNICAL 5SRV1C6 INC
-ORGANICS ANALYSIS OA7A SHEE7 . Page 3
/,cr: No: 1Q ^ 8
w i J
r ~- \ SambTe .
0' -?Y : 80106
luiroer |
i
I
«•••»... < i
CCMP'a'NO
Benzene - d5
j t (Surrogates arny) \
\ I Spue 1 * :
Fraction : Conc.(uo/l) ! Added (uo/1) i Recovery !
VOA ! 52.3 i 50.0 !
1 l-Chlcro-2-3ror.crropane: VOA ' 47.2 i 50.0 }
'• Toluene - d8
2-?luereshencl
Phenol - d5
1 Nitrobenzene - d5
2-?lucrobirhenvl
VOA ! 66.3 ' 50.0 1
ACID : 0 1 96 |
• ACID : 0 . i 106 I
3/* ! 188 ! 103 1
3/N ' 65 1 103 |
* due to high matrix Interfemece : j
8.
CAS 1 CCMPOU
7IN7A7IYE1Y i:5NT!?IED CC!-PC
-------
W65T COAST TECHNICAL S€RV1C6 INC INDUSTRIAL CATEGORY
SAMPLE ID 30107 WELL ?7
LA3 ID 1S601Y13
DATE INJECTED 6/21/30
STD ID OFTPP1C53 19600V4
CONC. FACTOR 5
Volatiles
2V acroiein
3V acrvlenitrile
4V ber.zsr.e
5V carbon tetrachloride
TV chlsrober.zsr.e
10V 1.2-dishlorse:har.e
11V 1.1. l-trichloreethane
13V 1.1-dichloreerhane
14V 1.1.2-trichlorcethane
15V 1 . 1 .2.2-tetrachlcrsethar.e
J 1SV chioroethane
inXXXXIXX;iM:ai(a;f^iXJCCX:^tti
-------
WEST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY.
SAMPLE
30107
.30 frf.39 SAMPLE ID 30107
LAB 10 19601A13 '".
^7E EXTRACTED 6/5/80
DATS IN'IECTED 7/7/80
S7D ID DF7PP1067 PHEN 245 -
COMC FACTOR ~ 20
Acid Cer.ocunds
21A 2.1.6-trichlaraohenol
T2A o-chlcrs-r.-cresal
2£A 2-chleraoherel
31 A 2.1-d:chlarcohenel
3^A 2.i-dir.ethvlohep.ai
57 A . 2-nitraoher.al
5cA i-n:trcoher.el
59A 2.1-dinitrcohenel
60A i.S-cir.itra-c-cresal
. e£A oentachlarcohencl
i&A 9henol
9
3ase/Veutral Canoounds
13 acsnaahrhene
53 ber.zidine
33 1.2.i-;richicrcben2«r.«
93 hcxachlsrrbcr.zene
123 h«xachlsrs*:har.«
153 btsi2H:hiorsethvUecher
2C3 2-chlorsna3thal«r»«
253 1.2-dichiorob«nztne
263 1.3— iichlorcbenzen*
273 l.i-dichlorobenzer.e
2SB 3.3f-dichlorsbenz:d:n«
353 2.1-dinttrataiuer.e
363 2.5-c:r.i:r5tcluer.« A ' 4
^B 1 . 2-diphenylhycraz:ne
''as azcber.zsr.e)
393 fluorar.th-r.e
ug/1
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
3935
NO
NO
NO
NO
NO
HO
NO
NO
NO
MO
NO
NO
MO
NO
NO
£C3 i-chisrsohep.vl ?her.vl ether NO
LAB ID 19601310
DATE EXTRACTED 6/14/80
DATE INJECTED 7/13/80
STD ID OFTPP1073 3NSTO 275
CONC FACTOR 50
Base/Veutral Csmoounds - u
ilB ^-bromoohenvl ohenvl ether
i2S bi3(2-chlsr3tscorcovl) ether
£33 bis (2-chlarsechoxv) methane
52B hexachlarabutadiene
53B hexachlorocvclcoer.tadiene
5^8 isaohcrsr.e
553 naohthalene
563 nitraber.zene
6iB N-ni:rcscc:r.ethvlasiine
623 N-ni:rascci3her.vlar.ine
63B M-nitroscdi-n-oreovlamtne
6eB bis (2-ethvlhexvl) ohthalate
67B butvl ber.zvl ohthalate
66B di-n-butvl ohthalate
69B' dt-n-cc:vl ohthalate
70B diethvl ohthalate
713 dirr.etr.vi ' ohthalate
729 ber.za'ia) anthracene
73B benzciaJovrene
713 3.i-benzcP.uaran:hene
75B benzot JOfluoranthene
763-- chrvsene
77B acenaohthvlene
78B anthracene
79B benza'. shi-oervlene
303 fluarene
513 ohenanthrene
S23 dibenza1. a. h) anthracene
333 indenc- 1.2.3-cdJovrene
Si 3 avrer.e
I2?B 2.3.7.S-tetrachiaradibenzo-
- •
g/1
NO
NO
NO
NO
NO
NO
NO
107
NO^
NO
NO
NO
NO
NO
35
NO
214
NO
MO
NO
NO
Mp •
NO
NO
Np
NO
"3
•JO
in
MQ
•diaxin
-------
W6ST COAST TECHNICAL S€RV1C6 INC.
ORGANICS ANALYSIS DATA SHEET - Page 3
Xcort No: 10
fi
*9ue
r.%
41
to
0^2?
H1gn Matrix
Interference
| Sample
! 30107
Nurroer
A.
;
COMPOUND
Fraction
Conc.(uo/1)
1 i Surrcoates only I
j Spue • 5
I Added (ua/1) ! Recovery
Senzene - dS
VOA
50.3
50.0
101
l-Chlcrc-2-3rcrsrrorar.e
VCA
45.7
50.0
90
Toluer.e - d9
VOA
I 55.8
50.0
111
2-?luoroeher.ol
ACID
143
108
| -132
Pher.oi - dS
Nitrobenzene
- d5
1 ACID 1
' S/N 1
NO
450 .
1 105
i 103
i o
! 437
k
1*
2-?lucrobirher.vl
48
103
46
;!5.
n
17. '
3. T-NTATIVS'.Y i:zN'!?IE2 CC
i
CAS
1 COMPOUND NAME
FRACTION
• Maximum Score Attalnea
Mass Matching Routine: FIT
TSecTTy 1 :
11.
*. i
3. i
*. :
:5. '
'5. :
.7. !
:8.
*. i
'*o •
in. :
'•12. '
U, i
ij. •
IDICHLOROFLUORCMETHANE VOA#71
! UNKNOWN
J2-PROPANOL
VOA487
VOA^IOI
il-PROPANOL ! VOA¥122
2-3UTA.NOL
VOAi>175
973
NO GOOD FITS
980
969
939
J1-3UTANOL i VOA*206 978
i UNKNOWN
VOAf241 ; NO GOOD FITS ' \
ETHYLESTER6UTANOICACID ! VOA^347
l^EXANOL
VOA*374
976
985
2.3.4-TRIMETrfYL HSXANE; VGA-439 • 919
IUNOCWN ' AC! Of 51 NO GOOD FITS
•UNKNOWN ; ACID-53
i UNKNOWN AC 10*75
NO GOOD FITS
NO GOOD FITS
:i4. i iUNKNCWN^^- ^ ; ACID-102 NO GOOD FITS
!15. '
i UNKNOWN i AC!D*130 ; NO GOOD FITS
:IJN:<::CWN
ACIO»i34
NO GOOD FITS
:!JNK,NCUM
ACIO-15Q i NO GOOD FITS
;NCNANOIC ACIO
ACI>139
953
:*o
i «.,,—.,.. ». .«,«..
• ^C '-«*.-« fv.i
334
-------
W€ST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY.
SAMPLE ID BO 108 .
LAB ID 1960811
DATE EXTRACTED 6/U/80
DATE INJECTED 7/13/80
STD ID DFTPP1073 3NSTD275
A
SAMPLE ID 30108 ^fi^h ib
LAB ID 1960A10 £$- 22
^TE EXTRACTED ~ 6/15/30
DATE INJECTED 7/7/80
STD ID OFTPP1067 PHEN245 -
CONC FACTOR 1000
Acid CsT.oounds
21A 2.£.6-trichloroohenol
22A ?~-h:src-?-.-cTesc!
2£A 2-chloreohenol
31A 2.i-dichlsrcohenol
3£A 2.£-dir.e:hvlohenol
57 A . 2-nitroor.enol
53A i-r.itrooher.ol
59A 2.i-dinitrcohenoi
£CA i.6-dini:rs-c-cresal
o£A oentachlcroohencl
j^ ohenoi
Base/Neutral Comoounds
13 acer.aohthene
53 bep.zidip.e
33 1.2.£-trichlarsbenzer.e
93 hexachlsrsbenzene
123 hexachlorsethane
133 bis(2-ch!ersethvl)«!he?
203 2-chloronaothaltnc
253 1.2--dichicrsb«nz«ne
253 1.3-dichicrobenz«ne
2T3 l.i-dichlcrsbenzer.e
233 3.3'-dishlcrobenzidi'n"e"
3«3 2.i-iinitrotcluer.e '
363 2.f-ciir.i:r3toluene . • _>
^B '.,2-dioher.yihydraz:ne
3?3 f'.usrar.ther.e
^C 9 ^^*i» *»»W»^W^S**VL j .•*»•» '» «•••(
So/ n
cf 3i
ug/l
NO
MQ '
NO
NO
NO
NO
NO
NO
NO
NO
NO
*
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
MO
'10
NO. '
MO
!-!0
CONC FACTOR
1000
Base/Neutral Comoounds . ug/l
£13 £-bromoohenvl ohenvl ether NO
bis(2-
) ether NO
£33 bis (2-chloroethoxv) methane*
523 hexachlcrobutadiene NO
533 hexachlorecvclcoentadiene NO
543 isoohcrone NO
553 naphthalene 13
563 nitrobenzene NO
613 N-nitrosodimethvlanir.e NO
623 N-nitrosoaiohenvlamine *
633 N-nitrosodi-n-proovlamine NO
663 bis (2-ethvlhexvl) ohthalate NO
673 butvl benzvl ohthalate
683 di-r>-butvl ohthalate
693 di-n-cetvl ohthalate
703 diethvl ohthalate.
713 dirr.ethvl oh;halate
728 benzo(a) anthracene
733 benzo(a)ovrer.e
7£3 3.£~benzofluoranthene
753 benzo(k)fluoranthene
763-. chrvsene
773 acenaohthvlene
783 anthracene
793 benzo''ghi)oervtene
SOS fluorene
813 ohenanthrene
325 dibenzoia.h)anthrace-ne
333 indeno{1.2.3-cd)ovrer.e
3^3 pvrene
1293 2.3.7,3-cetra.chlar5d:benzo-
o-dipxin .
NO
.NO.
JSL
67
NO
MQ
NO
MD
10
vn
yn
_NO_
NO
NO
co-
-------
WEST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
•fr
6/21/80
SAMPLE ID 30108
LAB ID 19601VI3
DATE INJECTED.
STD ID DPTPP1054 19601V15
CCNC. FACTOR
Volatile*
2V acrolein
3V
acrv'.3r.i:rtle
LV benzene
6V carbon tetrachloride
£3V dichlorrbrcrcmethane
£9V trtchlgrgfluoramethane
50V dteh:grgdif!uorgrr.e;hane
51V chlgrgdibrorr.cr.ethane
55V tetrach'argethvlene ^^
5SV vxnvl chloride
ug/1
JIO
_NO
_57
NO
10V
11V
13V
UV
13V
16V
1 . 2-dichlersethane
1.1. 1-trichlorsethane
1 . 1-dichloroethane
1.1. 2-trishlcrsethane
1 . 1 . 2. 2-tetrachloroethane
chlorcethane
NO
NO
NO
NO
NO'
*
19V 2-chloroethvlvfnvl ether NO
23V chlorofora Ng_
29V 1.1-dlchlcroethvlene ND_
30V 1,2-trans-diehlcroethvlene 11
32V 1.2-dichlorgprooane
33V 1.3-dichlereorgo vlene
38V ethvlbenzene
LLV aethvlene chloride
15V aethvl ehlortdt
i6V r.ethvl bror.idt ._
NO
40
NO
MO
NO
NO
—112.
325
NO
SAMPLE ID 301 08
LAB ID TRACE *578. 573. 575, 604
DATS EXTRACTED 6/14/80
DATE INJECTED 6/24/80
STD ID TRACE ?604
CCNC. FACTOR ' 100
Pesticides
89P aldrin
90? c:eidr:n
-91? chlerdane
92? £.r-DDT
93? £.r-DDE
- Ug/1
NO
NO
NO
NO
NO
9L? *.*t-DDD NO
95? aloha-endcsulfan
96? beta-«ndosuifan
97? er.dcsulfan suifate
98? endrtn
99? endrtn aldehvde
100? heotaehlor
•101? heotachlor eocxide
102? aioha-BHC
103? beta-8'HC
10£? camna-SHC
NO
NO
MO
NO*
NO
NO
NO
NO
NO
NO
105? delta-BHC NO
106? PC3-1242
107? PC3-1254
108? PC3-1221
109? PC3-1232
HOP PC 3-1213
111? PC3-1260
112? PC3-1016
113? toxaohene
NO
NO
NO
NO
NO
NO
•JO
'10
* • Less than 10 ug/l
(pesticides less than 5 ug/1)
ND • Not detected
•* « Not con/imed by CCMS
A-23
-------
-WEST COAST TECHNICAL SERVICE INC
ORGANICS ANALYSIS DATA SHEET - Page 3
vo;
10
&&241
NO GOOD FITS j
NO C-CGO FITS S
2,5-OI*ETHYl 3UTANOIC ! ACI>2S5 .
13.
;ci>273 : 895
•10
-------
Wteb. LUAb. TECHNICAL S€RV1C6 INC. INDUSTRIAL CATEGORY.
SAMPLE ID BO 109
SAMPLE ID 30109
LAB ID 19601A11 fK.t*!i«Mi frM
DAT! EXTRACTED 6/15/30
DATE INJECTED 7/7/80
STD ID OF7PP1067 PHEN245
CONC .-ACTOR 1000 '
*
Acid Compounds ' u
21 A 2.i.6-trichiorcohenoi
22A o-chlors-rs-crescl
2-A 2-chlorsohep.ci
31 A 2.1-dichlcrct>henel
3*A 2 . 1-di.r.ethvl3her.ci
57A 2-nitrsoher.oi
5»A i-nitrsoh«r.oi
5?A 2.1-dir.i:rraher.ol
6CA £.5-d:nitrs-o-cresoi
e£A Dcnrachlsrcrher.ol
55 A ahcnol
3ase/Neutrsl Compounds
13 acsnashthene
53 benzidine
S3 1 . 2. £-trtshisr9bt r.z«n«
93 hexachlcrcbcnzene
123 hexachlsrrethane
1S3 bis(2-ch!ors«!hvi)tth«r
203 2<-chlorona9thmltn«
253 1 . 2-dichlorcb«ft2tnt
253 1.3-dichlersb«nztnt
273 l.i-dichlorsb«r.zent
253 3.3'-di=l:'jp-!'v.sn^^:R«
353 2.i-dini:r3toiuep.«
* * 3 *% * • •
.•09 ^. o-u... ...•;•. \.:ue.i«t
373 1.2-d:ph«ny'.hydraz:»^^' •*
'as azsbenzsne)
:?3 r.«ra.-.:.-.«r.ft
iC3 i-chlsrsorenvi op.er.v; *:r.er
*f -L
^^^^^^••^^
g/1
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
*
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
MO
''V
MO
•in
«jp
LA3 ID 19601812
DATS EXTRACTED 6/14/30
DATE INJECTED 7/13/80
STD ID 3NSTD275 OFTPP1073
CONC FACTOR 1000
Base/Neutral Compounds u
^13 ^-brsr.oohcnvl ohenvl ether
i23 bis(2-chicretsoorsovl) ether
£33 bis (2-chloroethcxv) rr.ethane
523 hexaehlorobutadiene
533 hexachlorocvcicoentadiene
5^3 iscnhcrone
553 naohthalep.e
563 nitrsbenzene
613 M-ni:rosodi.T.ethvlas!ine
623 N-nitrsscdishenvlamine
633 N-nitrosodi-n-oroovlaraine
663 bis (2~«thvlhexvl) ohthalate
67B buevl bensvl ohthalate
663 di-n-butvl ohthalate
693 dl-n-cctvl ohthalate
703 diethvl ohthalate
71B dincthvl ohthalate
723 benzo(a) anthracene
733 benzol a) ovrene
7^3 3.^-benzofluoranthene-
75B benzo(k)fluoranthene
763 chrvsene
773 acenaohthvlene
733 anthracene
7?3 be;izc' shtJaervlene
503 fluorene
313 ohenanthrene
523 dibenzo(a.h)ap.thracene
533 indenoil.2.3-cd)ovrene
5-3 ovrene
1293 2*3.7,5-tetrachlorodibenzo-
*
g/1
NO
MO
NO
NO
NO
NO
NO
NO
NO
NO*
NO
NO
NO
*
NO
NO
MO
NO.
MO
NO
MO
MO .
NO
MO
NO
Nf»
«tn
vn
MD
MO
3-dicxtn
-------
W€ST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
SAMPLE ID BOT09
LAB ID 19601V19
TE INJECTED
p ID DFTPP1Q54
CCNC. FACTOR
Volatiles
2V aeroiein
rftf '3
" 5/21/80
T960V/15
S7V
- -—v1 -*•*»
.*s«• * •«»•••
benzene
...•t.
6V carbon tetraehierlde
TV
19V 2-chIargethvlvinvl ether
23V chloroform
LLV ffiechvlene chloride
nethvl ehlcridt
T.ethvl
LT1 bromofora
£9V trichlcrafluofga«thant
50V diehlorcdtr.uargr.ethane
• • ~ « mmmftrm «/• <»••*
• ^.••^» ^C»««V«C.-C
ug/I
NO
MO
ND
NO
NO
10V.
11V
13V
UV
15V
16V
1.2-dichlsrsethane
1 . 1 . 1-trichlorcethane
1 . 1-dichlercethane
1,1. 2-?richleroethane
1.1.2. 2-tetrachlcroethane
ehlorcethane
NO
NO
NO
NO
NO
NO
NO
N0
30V
32V
1 . 2-tra'ns-dichlsrseth vlene
1 , 2-dichloroorooane
NO
NO
33V 1.3-d:chlsrct>r3ovlene NO
38V
ethv'.benzene
NO
S8V vi-.v: chloride
NO
NO
NO
NO
NO
ND
SAMPLE ID BO 109
LAS ID TRACE «70
DATE EXTRACTED 6/14/80
DATE INJECTED 6/24/30
STD ID TRACE -571
CGNC. FACTOR 100
Pesticides
89? aldrtn
9CP cialdrin
91? chlordane
92? 4.4'-DDT
93? 4. 4 '-DDE
94? 4.4' -ODD
95? aloha-endosulfan
96? beta-endosulfan
97? endosulfan sulfate
.uq/1
NO
. NO
MO
NO
NO
NO
NO
NO
NO
98? endrtn NO*
99? endrin aldehvde
100? heotachlor
101? heotachlor eooxide
102? aloha-3HC
105? beta-3HC
104? ?anma-3HC
105? delta-3HC
1C6? PC3-1242
107? PC 3- 1254
108? PC3-1221
1C9P PC3-1232
HOP PC3-124S
111? PC3-1250
112P. . PC3-1016
113? roxaohene
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
* • Less :han 10 ug/l
(pesticides less than 5 ug/l)
ND - Not detected
•• • Not canfiraed by GCMS
4
A-26
-------
g? W65T COAST TECHNICAL S€RV1CS INC
- OR6ANICS ANALYSIS DATA SHE-T - Page 3
t No: 10 ft 176-21
Sample Nusioer
301C9
A. SU3RCC
CCMPCUNO
Fraction
1 (Surrooases oniv) :
Conc.fuo/1)
1 Splice
! Added (ua/1 )
*
Recovery
Ser.ier.ft - dS
VGA
50
SO
100
l-C.w.loro-2-3roTr.ogrogar.e
VOA
45
50
i SO
Toluer.a - d2
VOA
53
50
i .106
2M?* •««*4»0*MUA*»*O
• • «•«•• *» W«*C«*W«
ACID
I 84
108
78
i Phasol - d5
ACIC
77
105
2-?luerebi3her.vl
54
TOT
i 73
1
sr.e - d5
' 3/N
! 55 •
; 103
I 55
9. TENTATIVELY IDENTIFIED COMPOUNDS
1 : '
I CAS 1
COMPOUND NAME
FRACTION
2 Maximum Score Atulnea
Mass* Matching Routine: Fl?
(soecifv
• ,
i. ! (UNKNOWN
2. ! JTRIMETHOXYMETHANE
VOAI57 | NO 6000 FITS |
VOA#195
3. ! . {UNKNOWN i
4. i I
OI3UTYLEST£R-I,2- \
927
NO 6000 FITS
s. ? IBENZENEOICARBOXYLIC AciJDjAcio*257j 943
6. i :
UNKNOWN ;' B/N§247 | NO 3000 FITS
7. , (UNKNOWN
8. i f
9. !
B/N»306
NO 600D FITS 1
-. i i
•
1
'13.
.4. !
i i * !
SlS.1 * • i ! •
15. :
•17. ! !
Na : i
4, !
i 1 • 1
. i . l
-------
W65T COAST TECHNICAL S6RV1CE INC. . INDUSTRIAL CATEGORY.
SAMPLE ID 30110
Pool Q SAMPLS ID 30110
LA3 ID 1960A12 pgO
^7E EXTRACTED 6/15/30
DATS INJECTED 7/7/80
STD ID DFTPP1067 PHEM245
C2NC FACTOR 100
Acid Corr.oounds
21 A 2.i.6-trichlorsohenol
22A o-cr.lcrs-.r.-cT.asol
2L\ 2-chloroohenoi
31 A 2.£-dichloroohenol
3£A 2.£-dirr.ethvloher.ol
57A 2-nitrsohenol
5cA £-nitrsohenol
5?A 2,i-dinitrcohenol
60A i.5-dinitre-B isooherone 4572
553 naohthalene
563 nitrobenzene
613 S-nitrssodi.-nethvlar.ine
623 N-nitrosodiohenvlamine
63B N-nitrosodi-n-oroovlamine
66B bis (2-ethvlhexvl) ohthalate
673 butvl benzvl ohthalate
68B di-n-butvl ohthalate
693 di-n-cctvl ohthalate
NO
NO
NO g
NO
NO
NO
NO
*
NO
706 diethvl ohthalate 185
718 ditnethvl ohthalate
72B benzo(a) anthracene
738 benzo(a)ovrene
7£B 3.^-benzsfluoranthene
753 benzoik)r»uoranthene
763-- chrvsene
77B acenaohthvlene
783 anthracene
79B benzoiahiJoervlene
308 P.uorene
313 " ohenanthrene
323 dibenzo(a.h)anthracene
333 indencil.2.3-cd)ovrene
3^3 pvrene
U
NO
MO
NO
MO
MQ
NO.
NQ
N.D
NO
Mf)
N,P
N.H
NO
^-chlorcohenvl oher.vl etherMP
12$3 2.3.7.8-tetrachlorcdibenzo-
A-28
NO
-------
WEST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
80110
%
i
:.A3 ID 19501V20
3A7S INJECTED _
570 ID DF7PP1054
CCNC. FACTCR _
Volatile*
2V acrclein
6/21/80
IS601Y15
LV
acrylonttr;le
benzene
6V carbon tetrachloride
16V ehloroethane
17V bis(chloromethvl) ether
19V 2-chlorgethvlvinvl ether
23V ehlcroforin
29V 1.1-diehloroethvlene
30V 1.2-trans-diehlorgethvlene
32V 1.2-dichloroor3oane
33V 1.3-dichlgrgorgovlene
38V ethvlbenter.e
LLV ffsethvlene chloride
£5V siethvl chloride
ntthvl bromide
brsnoforn
dlchlorsbreff.orr.ethane
50V dtchlorodifluerortethane
51V cr.lor
35V tetraehlsreethvlene
5eV toluene
5TV tr'.shlorgethvlene
5SV vtr.vl chlor-.de
ug/1
NO
ND
53
23
10V
11V
13V
uv
15V
1 . 2-dichlorcethane
1.1. 1-triehlorgethane
1 . !-dlchloreethane
1.1. 2-trichloroethar.e
1 . 1.2.2-tetrachlorgethane
NO
11
199
NO
NO
20
,Np_
NO
NO
32
NO
25
475
27
NO
NO
76
20
ND
10
ID
•ID
SAMPLE ID 80110
LAB ID TRACE *605
DATE EXTRACTED 6/14/80
DATE INJECTED 6/25/80
STD ID TRACE *603
CONC. FACTCR 100
»
Pesticides
89P aldrin
9CP cielcrin
91? chiordane
92? £,r-DDT
93? £,r-DDE
ug/I
NO
ro
NO
NO
NO
94? £..£»-DDD NO
95? aloha-endosulfan
96? beta-endosutfan
97P endosulfan sulfate
98P endrin
99P endrin aldehvde
100P heotachlor
101P heotachlor eocxice
102? alpha-BHC
103P beta-3HC
NO
NO
NO*
NO
NO
NO
NO
NO
NO
10£P ?amna-3HC O.?!1
105? delta-3HC
106P PC3-12£2
107? PC3-125I
NO
NO
NO
108? PCS-1221 MH
109P PCB-1232
HOP' PC8-12IS
111? PCS- 1260
112P PCB-I015
113? toxaohene
MG
NO
MO
NO
NO
* • Less than 10 ug/1
(pesticides less than 5 ug/l)
MD • Mot detected
cgnfirsied by GCMS
••
A-29
-------
WEST COAST TECHNICAL SERVICE INC
-CRGANICS ANALYSIS DA*™ SHEET - Pace 3
•S.VQ; n PS ,±0flf 3l
•Matrix 1nt»r-fefrence with Isophrone
j Sample Numoer
|. BOTIO - j
/*-• —
CCMPCUNO !
; Senzer.e - dS !
• l-Chloro-2-3reiRooroDane
Toluene - d8 ~" !
! 2-Flaorosher.oi '
Phenol - dS S
Nitrobenzene - dS '
A. SURROGATE
J
Fraction ••
VGA !
VGA !
VGA !
ACID 1
ACID :
3/S '
SP.IXE RESULiS
Conc.fuo/11)
48
42
49
93.1
NO
1423
(Surrooa'es only) i
Splice 2
Added (uo/1) Recovery
50 96
50 84
50 1-98
108 86
105 0
103 1382 f
2-?luorobiohenvl
74
103
72
111.
B. TENTATIVELY IDENTIFIED COMPOUNDS
• i
i. i
^
3. i
4. ;
5. I
6. i
7.
8. '
9.
1 CCMPCUNO NAME
__
1 CHLOROFLUORCME7HA.NE
UNKNOWN
! 2-PROPANONE
1,r-OXY3ISE7HANE
UNKNOViN
j 1-oUTANOL i
i 4^CTHYL-2-P£.VTA?lO?lE
i 4-HE7KYL-2-PENTANOV
! 1-HEXANOL
FRACTION
VOA^30
YOA*68
VOA*85
VOA* U4
VOA#173
VOA#203
VOA/302
VOA*319
VOAf372
S Maximum Score Attained
Mass Matching Routine: FIT
i soecTTyT:
954
NO GOOD FITS
948
988
NO GOOD FITS i
977 i
953
955
969 !
UNKNOWN
i VOA»253
r ny
i UNOCWN
I ACI0455
NO GOOD FITS
i UNKNOWN
NO GOOD FITS
, UNKNOWN c_
ACIO?82 ! NO GOOD FITS
UNKNOWN
i AC!0«n06 i NO GOOD FITS
UNKNOWN
AC!D»122
NO GOOD FITS
UNKNOWN
ACIO*142| j NO GOOD FITS
NCNANOICACID
904
•i
73. '
: SENZOI-:
-------
W€ST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
SAMPLE ID B0111
feo/B
SAMPLE ID BOm
LAB ID 19601A14 ~> £\
DATE EXTRACTED 6715/30
DATE INIECTED 7/7/90.
STD ID DFTPP1067 PKEN245
CCNC FACTOR 1000
Acid Compounds
21A 2.4.6-trichloroohenol
22A o-chlcro-m-cresol
24A 2-chlors-phenol
31 A 2.4-dichlorcpher.ol
34A 2.4-dire'hvlohenct
57A 2-nitrophenoi
53A 4-nitrcp'r.enol
59A 2.4-dinitreohenol
5CA i.5-dinitro-o-crescl
64A oentachlorophenol
€5A ohenol
Base/Meutral Compounds
*
IB acenaphthene
53 benzidine
33 1. 2. i-?rlchiorc benzene
9B hexachlorcbenzene
123 hexachloroethane
133 bis (2-chlcrcethvl) ether
20B 2-chloronapthal«nt
253 1.2-cichlorobenzene
263 1.3-dichlerobenzene
27B 1.4-dichlorobenzene
2SB 3.3'-dichlorobenzidine
353 2.i-dini:rotcluene
363 2.5-dinitrstsiuene %*
373 1.2-diphenylhydraz:ne
•'as azsber.ser.e^
393 r.ueranthene
af .77
—
ug/l
NO
NO
ND
NO
ND
NO
ND
NO
NO
ND
159
•
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
NO
MO
NO
MO
NO
LAB ID 19601816
DATE EXTRACTED 6/14/30
DATE INJECTED 7/13/80
STD ID DFTPP1073 BNS7D275
CCNC FACTOR 1000
Base/Meutral Compounds ' ui
413 i-bromoohenvl ohenvl ether
423 bis(2-chioroisooreovl) ether
43B bis (2-chlorsethoxv) rr.eth-ane
523 hexaehlorobutadiene
533 hexachlerscvclspentadier.e
54B tsophorone 21
553 naphthalene
563 nitrobenzene
613 M-nitrosodir.ethvlaT.ine
62 B N-nitrosodiphenvlanir.e
63 B M-nitrosodi-n-propvlamine
663 bis (2-«thvlhexvl) ohthalate
673 butvl benzvl ohthalate
663 di-n-buivl ohthalate
693 di-n-octvl ohthalate
70B diethvl ohthalate
713 dinethvl ohthalate
723 benzo(a) anthracene
73B benzo( a Jovrene
74B 3.4-benzofluoranthene
753 benzo(k)fluoranthene
763 chrvsene
773 acenaohthvlene
783 anthracene
793 benzo(ghi)perviene
303 fluorene
313 phenanthrene
323 dibenzei a. h) anthracene
S3B indenei:.2.3-cd;3vr8r.e
343 Svrene
g/1
NO
NO
NO
ND
NO
121
ND
ND
NO*
NO
NO
NO
NO
NO
NO
34
NO
NO
NO
NO
NQ
NQ
NQ
* (
NQ
NO.
*
NO
'ID
NO
103 i-chlorsoher.vl or.envl etherjfl
129B 2.3.7,3-tetrachlorcdibenzo-
-------
W6ST COAST TECHNICAL S€RV1CE INC INDUSTRIAL CATEGORY
SAMPLE ID SOT"
LA3 ID 19601V22
TS INJECTED
D ID DPTPP10S4
CONC. FACTCR_
6/2T/80
19601VI5
Volatiles
2V aerolein
jV acrylcni:r;le
£V benzene
6V carbcn tetrachlbride
TV chlargbenzene
1CV 1.2«dtehlersethane
117 1.1.1-trlehlorgethane
13V 1. l-dichlcrsethane
UV 1.1.2«i7lchlcrcethar.e
15V .1.1.2.2»tetraehloroethane
16V ehlsroeihane
51V
32V 1.2-dichlarsorsoang
33V I^-dichlgraoraovlene
33V ethvlbenzene
LCI fr.eihvlene chloride
i5V ?nethvl chlarid*
ioV r.ethvl brcr.id»
-LT' brsr.ofars
iSV dichlersbrar.emethane
tr'.shiarsr.uorgrr.ethane
?C-V d:ehlcrs
tetracr.ljrcetr.vlene
ug/1
NO
NO
NO
NO
—
NO
19V 2-chlorgethv!vtnvl ether NO
23V ehlaroforn N0_
29V 1.1-dichlaraethvlene N0_
30V 1.2-trans-dichlaraethvlene 178
NO
NO
124
12
NO
NO
NO
NO
.MO
NO
NO
SAMPLE ID BOH!
LAB ID TRACE ?608
DATE EXTRACTED 6/14/80
DATS INJECTED 6/25/80
STD ID TRACE *6Q9
CONC. FACTOR ™Q
Pesticides
89P aldrin
90P dieidrin
91? chlordane
92P *.-r-DDT
93P £,r-DDE
ug/l
NO
NO
NO
NO
NO
94? £..£'-DDD NO
95? aloha-er.dcsulfan
96P beta-er.dasulfan
97? endasulfan sulfate
96P endrin
99? endrin aldehvde
1CCP heotachlor
101? heotachlor eooxide
102P aloha-BHC
103? beta-BHC
10£? aamma-BHC
105? del:a-3HC
106? PC3-1212
107? PC3-1254.
IOSP PC3-1221
109? PC3-1232
HOP PC3-124S
HIP PC3-1260
112? ' PC3-1016
113? toxaohene
NO
NO
NO
NO*
NO
NO
NO
NO
NO
2.7**
2.3**
NO
NO
NO
MO
NO
NO
NO
MO
•A
SSV vir.vl ehlcride
• • Less'th'an 10 u;/l
•
(pesticides less than 5 ug/l)
N'D • Not detected
•* • Not 'Ssnftracd by GCMS
4
-------
53 W65T COAST TECHNICAL SERVICE INC
-ORGANICS ANALYSIS DATA SH££T - Pace 3
X^.vo: 11 K 33 ^2cl
j Sample Nunaer
1 30111
/^~ A. SURROGATE SPIKE RESULTS
COMPOUND """"" -1 Fraction
' Ber.zer.e
1-Chlor:
Tol'— 6"fi
- d6 ! VOA
:-2-3renicsr3car.s VOA
- d3 - ! VOA
i 2-?lucro3henol 1 ACID
Pher.ol -
- dS ! ACID
Vitrebenzene - dS ' 3/tf
2-?lucrs
[
3bd.3h.snvl • 3/N
1
1 (Surrocates only)
1 SpUe i
i Conc.(uo/1) i Added (ua/1) Recovery
47
1 42
! 50
! 87
78
54
! 77
i
1 50 94
j 50 . 34
1 50 . -100
i 108 81
j 105 74
! 103 53
! 110 70
i
• »
8. TENTATIVELY IDENTIFIED COMPOUNDS
CAS
# COMPOUND NAME
FRACTION
S Maximum Score Attained
Mass Matching Routine: FIT
rSoecifv)
h.
2.
(3.
4.
5. i
5.
•7. •!•
:8.
9.
10.
11. :
12.!
13.
14.'
•15. •
15.
:17.:
13. i
'UNKNOWN
1 UNKNOWN
(UNKNOWN
UNKNOWN I
' UNKNOWN
UMUIOWK
UNKNOWN
UNKNOWN
UNKNOWN
! UNKNOWN
!2-PROPANONE
i2-PROPA^IOL- 4
' TrrRAHYOROF'JRAN !
I.T-OXYSIScTHANE-
: 2-SUTA;iCNE
• 2-3UTANOL :
! 4-METHYL-2-PENTANONE i
AC I 0*57
ACIDI88
ACI04113
ACIO'125
ACID^13S
NO GOOD FITS
NO GOOD FITS
NO GOOD FITS
NO GCCO FITS
915
ACID*144 : MO GOOD FITS '
ACIO*177 i NO GOOD FITS
ACItyi92
ACIO#217
AC I 0*223
VOA#85
VOAf83
VOAf98
VOA^129
VOA*U3
7CAfi574
VOA»172
VOA-3CO
NO GOOD FITS
NO GOOD FITS
. NO GOOD FITS
NO GOOD FTT?
970
i 977
! 983
I 968
932
953
; 979
-------
WEST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY.
SAMPLE ID 30112
/gg.r fctt/X
SAMPLED ID 80112
V
t3 ID 19601A17
TE EXTRACTED
DATE INJECTED
'STD ID OFTPP1069
CONC -ACTOR
~ p. 3£ ^f *
6/15/80
7/io/sa
PHENOL 25CA
1000
fj LAB ID 19601315
DATE EXTRACTED
DATE INJECTED
STD ID OFTPP1073
CCNC FACTOR
6/U/80
7/13/80
BNST0276
1000
Acid Compounds ug/1
21A 2.4.6-rrich:oroohenc! N0_
22A o-chlcro-m-crescl NO
24A 2-chIorsohenol
31 A 2.4»dichlercohenol
34A 2.4-dtT.ethvloher.ol
57 A 2-nirrsoher.gl
53A 4-nltrcohenel
5?A 2.1-dini:rcohenol
60A i.o-dinizrs-o-crescl
oentachlcroohenol
onenci
Base/Neutral Csr.oounds
13 acenaohthene
3/3 l,2-dipher.ylhydraz:p.e
•'as azs'ger.zene'-
393 r.ucranfr.ene
NO
N0
NO
NO
NO
141
NO
53
S3
93
123
133
203
253
263
273
283
353
•_
benzldine
r.2.4-trichlorobenzene
hexachlorsbenzene
hexachlorcethane
bis ( 2-chlorathvt )«ther
2-chlorsnaothalene
1.2-dichlorobenzene
1 ,3-dichicrobenzene
1 .1-dichlcr.-benzene
3.3'-d:chlorobenzidine
2.4-dinttrctcluene
2.5-din:trsto:uene
NO
NO
MO
NO
NO
NO
MO
MO
MO
MO
NO
NO
MO
MO
4C3 4-chlorsohenvl or.er.vl ether *?D
Base/Neutral Compounds uc/1
413
423
433
523
533
543
553
563
613
623
633
663
673
633
693
703
713
723
733
748
753.
76 3
773
733
79B
603
313
323
533
543
4-broraoohenvl ohenvl ether
bis(2-chloroisooroovl) ether
bis (2-chloroethoxv) methane
hexachlorobutadiene
hexachlarscvclcoentadiene
isoohorone
naphthalene
nitrobenzene
N-nitrosodir.ethvlar.ine
N-nitrosodiohenvlar.ine
N-nitrosodi-n-orco via mine
bts (2-ethvlhexvl) ohthalate
butvl benzvl ohthalate
di-n-butvl ohthalate
di-n-octvl ohthalate
diethvl ohthalate
dimethvl ohthalate
benzo(a) anthracene
benza(a)ovrene
3.4-benzofluoranthene
benzo( k ) flucranthene
chrvsene
acsnaohthvlene
anthr.c.ins
benzo( ihOoervlene
f'.uorene
ohenanthrene
dibenzo< a. h) anthracene
tndenoi 1.2.3-cd.'3vrene
m
ovrene
NO
NO
NO
NO
NO
NO"
NO
NO
MO
NO
NO
19
NO
*
SO
17
Mn
MP •
In
Mn
MO
MH
NO
n (D
NO
NO
n _m
NO
NO
NO
1293 2.3,7,3-tetr»chlcrsdibenza-
-------
• — • ——-«••• *. «• •• *^» it thrfw.* i ru^*w ^^M «wjwrv i
SAMPLE ID S01T2 ng 35 C
LAB ID 1960 1726
DATS INJECTED 6/21/80
STD ID DF7PP1C54 19601V24
rnvr ncT^B .....
Volatiles
2V acrolein
3V acrvicnitrile
iV ber.zer.e
6V carbon, tetrachiorlde
TV ch'.jrcber.zene
10V 1.2-dich!crs«t.k.ane
i?y 1 i l.ro.-t>l'c~»*;fca*e
iv/ ' 1-'J'e'i'e-^«'i-ai«
*^ V *«*vw*W«i«W*«»G»**• "*
55V :sluer.e
37V rr-.c.V.srserr.V.err* -
f OCi
-
Uff/l
NO
NO
NO
NO
*
NO
NO
NO
NO
NO
*
•
xxxx
NO
NO
NO
132
NO
NO
• •
40
*
NO
NO
NO
NO
«in
iiU
NO
NO
275
» '
SAMPLE ID B0112
LAB ID TRACE ?607 1 610
DATE EXTRACTED 5/W80
DATE INJECTED 6/25/80
STD ID TRACE *609
CONC. FACTOR 100
Pesticides
89P aldrin
90? dieldrin
ug/I
NO
NO
91? chiordane " M
92? i.i'-DDT
93? £.£f-DDE
NO
NO
9£? £.£'-DDD NO
9SP aloha-encosulfan
96? besa-«ndosulfan
97P endosulfan sulfate
96? endrin
99? endrin aldehvde
100? heotachlcr
101? heotachlor eooxide
162? aloha-3HC
103? beta-3HC
1G£P aamma-3HC
105? delta-3HC
1C6P PC3-12I2
107? PC3-125^
103? PCB-1221
109? PCB-1232
HOP PC3^12^3
111? PC3-1260
112? PCB-1016
NO
NO
NO
NO*
NO
NO
NO
NO
NO
NO
0.2**
NO
NO
NO
NO
NO
NO
MO
113P toxaohene NO
* « Less than 10 ug/1
(pesticides less than 9 ug/1)
ND -Not detected
•» • Sot csn/irsied by CCMS
vt.-.vl chloride
A-35
-------
S&g^ W6ST COAST TECHNICAL S6RVIC6 INC.
"QR6A.NICS ANALYSIS 2A7A SHEET - Page 3
•: Vo:
to'high Matrix Interference
Sample Numoer
- 80112
CCMPCl'NO~
3er.zer.a - dS
l-Chlsro-2-3rcSo-rror
Tolusr.s - d3
2-?luoreeh«nol
Phenol - dS "-,
yitrcber.rsr.e - dS
2-?luorobisher.vI
— j—
' Fraction Conc.(uo/1)
I VOA ! 50.2
>ane VOA ! 47.7
• VGA 48.0
! ACID 78
! ACID { 220
! S/N 138
1 ai
1
(Surrooates onlv) j
Spike . "m \
Added (ua/1) Recovery !
50.0 . 100.
50.0 95
50.0 95
108 72
105 509 , \
103 133
110 74 I
|
f
B. TENTATIVELY r&rir.*s CCMPCUNOS
I 2-PROPANONE
! VOA*86
968
! I • •
M».
COMPOUND NAME
FRACTION
•
% Maximum Score Attained
Mass Matching Routine: FIT
(soeciry)
i i
{3. i
S*. ?
:5. i
S. !
•7. '
:8. !
19. :
10. :
44 i
•12. '
"13. !
'14. i
•is. ;•
m-
•is. •
1 2-PP-OPANOL
1 TETRAHYOROFURAN
j 2-METHYL-2-PROPANOL
I 2-3UTANONC
1 2-3UTANOL
I 2-PENTANONE
1 4^ETHYL-2-PENTA,NONE
i 2-HEXANOL
1 UNXNCUN
! PROPA?IOIC ACIO
j UNKNOWN
j 8UTANOIC ACIO
* *
j VOA¥131 !
j VOA* 139 j
{ VOA* 160 i
; VOA*174 ;
1 VO/W242 i
j VOAf303 i
; VOAf320 j
! VOA*371 i •
i AC I 0*4 5 i
! AC I Of 57 !
j ACIOf62 j
, 2-METHYL-3UTANOIC ACIOi ACIOf71 |
! PENTANO& ACI3
i 2-METHYL-PSNTANOIC AC
: HEXAflOJC ACIO
•• UNKNOWN
I ACIDfSS •
ID ACIO-99 :
• ACIO?! 10 :
• ACIO-UV
946 '
985 |
924
907
953
936
954
915 ;
NO 6000 FITS 1
950
NO 6000 FITS
980
965
953 !
961
953
NO 6000 FITS f
'20. ;
A-3b
-------
W65T COAST TECHNICAL SfeRVltfe INC. INDUSTRIAL Q.A1
SAMPLE ID 30113 fifcSn*f
LAS !D 1S601A16 . ^ 37 ^3?
DATS EXTRACTED 6/15/30
DATS INJECTED 7/10/80
STD ID DFTPP1069 PHENOL 250A
CCNC FACTOR 1000
Acid Compounds
21 A 2.£.6-trichloroohenol
22A p-chloro-m-cresol
2iA 2-chlorsp'ner.ol
31 A 2.1-dichlgrgphenol
ug/1
NO
NO
NO
NO
3LA 2,£-dimethvlphengi NO
57A 2-nitrephenol
5SA £-nitrophenol
59A 2.1-dinitrophencl
50A £,5-dinitro-o-cresoi
e£A pentachlcrophenol
65A phenol
Base/Neutral Compounds
13 acenaphthene
53 benzidine
SB 1,2.^-trtchlcrgbenzene
93 hexachiorobenzene
123 hexachloroethane
153 bis'2-chloro«thvl)tth«r
203 2-
-------
W6ST COAST TECHNICAL SERVICE INC INDUSTRIAL CATEGORY
50113 5UMX
SAMPLE ID
A3 ID 19601V28
5/21/SO
511
5V_
S6V
'ATE INJSCTED^
STD ID OFTPPIOSA 19501V21
CONC. FACTOR
Vclaiiles .':
2V aerolein ^ ' • •
3V acrvlop.itrile
iV • benzene
6V carbon tetrachlcrlde
TV chlcrebenzene
10V 1.2-dichlorcethane
11V l.l.l-trichlcrsethap.e
13V l.l-dichlcrse:hane
UV 1.1,2-crichIorgtthant
15V 1.1.2.2-tetrach loroethane
,6V chloreethaae
19V 2-chloroethvlvirivl ether
23V chloroform
29V 1 . l-dichloreethvlene
30V 1.2-trans-dichlprgethvIene
32V 1.2-diehlcrcsr?,o.ane
33V l.S-diehlars-preg
38V ethvlbenzer.e _ 1
tnethvlene chloride
methvl ehlertdtl
aethvl brestidt.
17V bromoform 1 ^^
iSV dichlorcbrcr.o.fMihar.-'
I9V trichlorofluoroaethane
50V dichlorcdifluergrretharn*
ehlorcdibrgtr.or.eth4a>r^
tetrachlsrcethvlene
ug/I
NO
NO
ND
NO
HP
ND
NO
ND
ND
ND
NO
NO
N0
NO
NO
NO
NO
^ NQ_
NO
JI . . JS1D.
AT*x/ ?*•• ^ U U^^^^r »»
-------
CC Report Mo;
W6ST COAST TECHNICAL S6RV1C6 INC
JQRSANICS ANALYSIS DATA SHEET - Page 3
3
9 tff
e Numoer
30113
A. SlXSCGxTc 5?I.<£ RESULTS
I
1 ...:.'' COMPOUND
! 3er.zer.« - dS
Fraction
VGA
Cone.
54
! l--h-2rs-2-3rs-ccro=ar.e VGA ' ' 50
1 Toiuer.e - d3
VOA
52
! 2-?lucrooher.ol ! ACID 61
Pher.oi - 45
Nitrober.ser.c - d5
2-?l-or3birher.vl
ACID ! **
3/N ! 57
(uc/1)
.0
(Surrocatas cnT
Spue
Added (uc/1)
50.0
.3 | 50.0
.4
50.0
| 108
! 105
o
3/N 9S
103
103
v)
1 •*
*
1 Recovery
!
i
i
1
i
i
i
1
1
108
101
105
56
44
55
92
8. TENTATIVELY ISE.TIFISO COMPOUNDS
-
1.
2.
3.
4.
5.
5
w •
'_
8.
9. !
CAS 1
-
•
-
-
i
COMPOUND NAME
UNKNOWN
UNKNOWN
•
i
1
1
1
!
.."
FRACTION
B/NI384
B/Nfl40
.
2 .Maximum Score Attalneo
Mass Matching Routine: FIT
soecify)
.
NO GOOD FITS
NO GOOD FITS
i
10.
17.'
13. '
-------
^>£AM?LE ID METHOD 3 LANK
LAS ID 1S601A15 ~ , *(
DATE EXTRACTED V/15/80
«E INJECTED 7/10/80
'^
1D OFTPP1069 PHENOL 250A
. CONC FACTOR 1000
. Acid Ccnjocunds
21A 2,£,6-trichloroohenol
22A o-chloro-ra-cresol
2£A 2-chiorcohenci
31A 2.£-dichloroohenbl
3£A 2,£-dinetnvlohencl
57A 2-nitroohenol
53A £-nitroohenol
59A 2.£-dinitrcohenol
50A £,5-dinitrc-c-crssol
6£A oentachlcrcohenol
ug/1
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
55 A ohenol *
\A -
./^•se/Neutral Comoounds
13 acenaohthene ' '
53 benzidine
S3 l,2.£-trichlorcbenzene
98 hexachlorobenzene
123 hexachloroethane
153 bis \ 2-chloroethvl)«th«r
203 2-chicronaothalefte
253 1 , 2-dichlorsbenzene
.263 1.3-dichlorobenzene
^»J « / J< „•„».-•..!».«••••,_
&/ o i . — — cizniorcoenze_nj6
NO
NO
NO
NO
NO
NO
NO
NO
NO
-NO
•233 3.3'-dichlorcbenz.ldin« • • — W
333 2 '-dtnitr3tcluer.e_
363 2.5-dinitroteluer.e_ •
tfj& 1.2-di?henylhydr.&2ine
^^ 'as azcb«nzene'»
393 r.uorantr.ene -
£03 £-chi3rsoher.vl ohenvl e
NO
. -ND
NC
NO
therNO
SAMPLE ID METHOD BLANK
LAB. ID 1960134
DATE EXTRACTED 6/14/80
DATE INJECTED 7/12/80
STD ID DFTPP1073 3NSTO 275
CONC FACTOR 1000
Base/Neutral Compounds us
£13 £-bromoohenvl ohenvl ether
£23 bis(2-chloroisooroovl) ether
£33 sis (2-chlcrse:hcxv) r.e:ha-r.e
523 hexachlorcbutadiene
533 hexachlorocvclooentadiene
5£B isoohorone
553 r.abhthalene
563 nitrobenzene
613 N-nitrosodireethvlamine
NO
NO
NO
NO
NO
NO
NO
NO
NO
623 N-nitrosodiohenvlanjine !*1D
633 N-nitrsscdi-n-oroovlaisine
NO
663 bis f2-«thvlhexvl) ohthalate *
673 butvl benzvl ohthalate
683 di-n-butvl ohthalate
693 di-n-octvl ohthalate
NO
NO
NO
703 diethvl ohthalate NO
713 dinethvl ohthalate
723 benzo'a) anthracene
NO
NO
733 benzoi a )ovrene NO
7£S 3.£-benzor.uoranther.e N?
753 benzo(k)fluoranthene
763 chrvsene
77B acenaohthvlene
783 anthracene
793 benzo(5hi)oervlen4
908 • fluerene
&13 ohenanthrene
323 dibenzoi a. h) anthracene
333 inder.ofl*2.3-cd^vrene
d£3 ovrene
Nf)
NO
N.n
in
MH
MH
NO
NO
NO
1293 2.3,7,3-tetrachlorsdibenzo-
A-40
-------
~
•::MPCUNO
»a-ser.e - d6
3 WEST COAST TECHNICAL SERVICE INC
:SSA.N!CS ANALYSIS DATA SHEET - Pace 3
i Sample Numoer
n ^
-------
MM PIMM) AM ti
1'i.ujiti IIAHC MI •/.*•! iu i
MO
mip*
rn
•WOU.7V- tin/Of./11
or OCPIM IAHNII PAWN)
PAY
14?$ 1994.0 S?M»
II
V
*
VK'4.0
joo.toin.-)« PO/OI/II J-H'» uoi.o
OIOTY SIlVi.N
OIWI
010 U
0144?
II100'
OI-U1 MliRM
01 ^1? LNfllUKlV
01141
010*4
IIIIC
OlOTf SllVl*t
01 002 ANSC'IIC
01012 '•.CMVllll
01071 CApTlUtt
ll'»42 CIIPPIR
11400 ltrf
I0.0001
73.000I*
IO.OOQO
4.000M
ir.oooc
•OO.OOl*
.700000
10.0001
7.00000
•KOOOOO
.400000
110.00"
lo.ooo-:*
4.f0090
1C.0000
q.eoooo
9J.OOOO
'.OOOOH
.noooor
.400000
10.0000
4.00000
U.noor.
PI. -00*
.-.0-1001
.HOOOOil
.400900
J
R
R1
J
R
R
J
R
R
J
J
IT. /I C
u
u
II
u
u
I'
SO IN
4 50
OC
4|.» b
20.000
21.409.
24.IAQ
IJ.OP"1
20.010
6I.?;«0
*o.o:o
21.410
n««"<»
flllr-O
I.*.?--'
O. »
20.000
7oloOO
2I.4CC
IJ.$"0
29.409
24.100
2J.09J
70.0CO
.-o.ooo
."O.OO'I
,-o.onn
,-O.P-U»
-------
UU ;
PKttJtGV Nil? PRfntCTUN OlSPUSAt
9 STA
TiBe
Or DEPTH
OAV
LABNO PANNO
5T8io
00
ft
34*49
*46l?
14660
J9dil
34*95
1420*
39121
34554
39TOI
UNITS CHEMIST*V
4,ft-UINIIRO-U-CHESOL
PENrAtMtMttPHfNlIt "'
PliTHUt
ACINAPMTMENE
rENIIOtlir
142 T*
34504
34539
BISI?-CMtONUllHm ET.
34ST4
~1*«V
34*14
1,3-OICMlORtHiENIiln: '
|,4-|IICIN.IWMFNIC>«e
1. J »-U ItHtUfcuntMl I OlHF
IV
i
34149
' 34379
14*44
2,4-DlhirftOfOiUCHC ' '
I» 2-IU PMENUMWMIINE
4-CIH.nftOPHENU PMEIVt ET,
4-HtUHuptiEiw. wrtivi: rr;
3420*
342*1
34394
34)119
IK-XACIUIMfWUIAPIENt
lirxACNllWOCVCiUrlNTAOirNE
1
Jl
ft'
~)444f
34450
3444|
3443*
»*4)|
)9|02
h-llindSODlMCINVlAMlMl
N-NI TllllSIH>inM!NVLAM|.lE
TtlSI2-ETtmilEmi PNTNALe
>...
39112
34199 DI-N-OT.m PIIINALAlt
14119 UIFTMVl PNTNAIATC
34344' UIHtlHVl PHTNALAlf
34529 1.2-BEHIANIMRACFNE
-14M6-"llfmO A*i
II
ft
ft
1
ft
II
ft
34233 3t4-OFNiariUtmANTHCNC
3424f 11.12-f.eNtOf ilNMANTHEtff
34323 ClMVSENI
14201 ' UtNAPMlHvlSMC "
34223 AriTIMACLNC
•f4524-
343W4 ILflUilEHE
34464 PHENANIMMNC ~
34559 |«2 5.6-OIMN2ANIHMCCNS
PVMEME
344T2_PtPf.»IE
')4«lii tCfid "
OIOTO
UC/RG
UG/RG
UC/RG
UG/BG~
UG/RG
UC/RC
UC/RG .
UC/RG
ur./nc
UC/RC
UC/RG
UG/RG
UG/RG
UT./RC
UG/RG
'llC/fcC'
Ut/RC
SFOINrNf
SCOlNEHf
SCDINENI
UC/RG
UG/RC
UG/KG
UT./RG
UG/RG
UG/RG
UG/RG
I«/RO
INi/RG
UG/RG
UG/KG
UG/RG
llfi/RO
UO/RC
UC/Rfi"
UC/RG
UC/R6
IIG/RG
•Hi/RG
UC/RC
liC/kt •
UC/RO
UG/RG.
UC/RG
tW/RG
UC/RC
Uii/RG
UC/RC
IN./RG
UC/RG
UC/RC
UC/RC
UC/KG
MC/RC
SEOINCNr
SEOINCNT
SEOIMF.Nr
SFUlHt^t
SnilHCNf
SEOlNCNt
SEUINENI
SEOIHCNf
SCOIHFNr
SEOINCllt
SEDIMENT
StUlHttit
SEDINENf
SEOINEHI
SfcDINENT
SCttlKfHf
SEDIMENT
SCOIHfMr
SEOIMFNT
SEOIMTtlf
SEUIMCNT
SEUIMfNT
SEDIMENT
SEOINliit
SEOIMTNT
SEDIMfNI
SEDINtNT
SEDINTNT
SEDIMENT
SlOlNfiit
SEOIMtMT
SEDIMENT
SEDIMENT
SEDIMENT
SEOIMfNI
SlftlMCNf
SFOINCNT
SIOM«INT
SEOIMfNf
SEOIMlNt
SEDIMENT
.PMUJECT OAl^O/Of/01
VALUE ft REMARK SO OR • OC
U
U
U
U
U
21.0000
140.000
2200.0.1
110.000
50.0000
SEDIMFNT
SEOIMENt
SEOIMFNI
SEUlMENT
SrDlMCNT
SEDIMTNI
SEDIMENT
110.000
Iid.ooo
1*0.000
.000000
U
U
U
u
u
u
u
u
u
IT
u
u
u
u
•l)-
u
u
u
u
u
u
u
u
u
u
f
u
U"
u
u
u
u
u
u
u
u
u
J
20.000
20.000
20.000
-J61080"
20.000
20.000
20.000
'20.000
20.000
20.005
20.000
20.000
20.000
20.000
20.000
20!ooo
20.000
20.000
20.000
20.000
2o!oOO>
20.000
20.000
20.000
20.000
15.000
20.000
20.000
2O.OOO
2O.OOO
20.000
20.000
20.000
20.000
20.000
20.000
fO.
-------
pp.rijrr.i »KI tat
<
Uiif
r.'i -HI r-Mj*
TO
tin.
r:r IICPIM
IIAV
.. i
r'' i • i1 \ i • i. • o.'')
.:' % ' I I I' i
PAUMO
01001
oioii
oio/w
OlO?1
010*1
*iAir
OI09t
tr»n
•iKRU
ANIIMCIV
01011
191.11
I'M" I
11151
19101
ll«AtlHH«
flit
M.UNI'1
|:IILi.K|'{
I'M 1 1
14154
if vi I
*,4*-IMMI
AlfM
i-ru
tNIHl
r;N*iu
Aii»fMvi-t
19411
194^1
19016
AlPIU-flC
IIFIA-BIC
1476?
14.-62
rrii»-mir.
99491
VI4-»»
19501
PCf-l?6P, , ... ,
I-CI'-|««I6
194-n iniApiirrr ........ (. ,
147 if nriiir.ni
14799 tMtin icmacinn*'.|nr
i4 104 cin.imiiiii.rif rii.
945(11
14499
5
S
&
IIMM'
94519
)4t|4 CI'LHItll
147»l I'lSliMimiPTIIIVll 'I.
14519 X-CMilUvlirillVi Vll.VI. 'I.
14MI4
14549 it 7- IN Air. oict\ir rr iunr'ir
1454* I.J-i
14S64 1.1-UIClHUKUPNi:
IPIIIS
UG/M;
M./RG
M./M.
rr./rc
M;/» r.
H/m;
•V/M;
W./I.G
OC/RI.
ir./nt
it/Mi
UC/RC
nr./RG
UK/RC
UI;/RC
iiii/r.r.
uc/rc
Iti/RC
Uk/»Cl
UC/RO
UI./RG
UG/RG
Wi/rc
ur/rr.
IIC'/RC
lir./rr.
I'G/RG
UU/RG
UC/RC
IN;/RG
5€OIHC»II
SCHIMINI
SCO I •»•'!»
SI UI HI HI
sri'iMi u
SlOlMLHf
SfUINfll
Stb|H!l4T
MIHHV.'ll
StOINfUl
sci/ini MI
SCUI^IIf
SCDIHC'II
SCUINMt
SIDIH.NI
SIOINI.Ml
SfUIIKlll
Sr.iHM'.'ll
SFOinrnt
Sfium.il
sruimm
SIOIWII
scpimit
sruirtriT
sruinriii
Sf III Will
scuim*tf
SlDINlill
scuim-ii
sim K HI
stm mm
snunr.iir
SEUIINNI
StUINItll
UIHMfNI
SFMIM'II
"lf>l fiAfr
Mrt. f KM* i-o/oi/tn
Vtlllt t "« H«HH
6.IOOC4
1.0000(1 J
.looooo r
79.0000
7.10. cor
.50OOUO*-OI 9
160.000
I*.oooo
f>. roooo
.90COOO -«| J
.700030 R
II
u
u
u
u
u
u
II
u
u
u
u
II
u
u
u
u
u
u
u
u
u
u
u
u
ll
t;
u
u
u
It
u
w
u
II
V
V
u
u
..._„)
M» U«
P5P
1C
VAH II
70.010
2O.QUO
^o.ono
JO.ore
70.000
70.ore
70. on
70.0P4
fO.OOC
70. '••.•'•
ro.opc
.••o.o.-r-
7C.OM'
ro.oun
70.03-
70.000
70.01.
70.0^0
70.0"C
7P.rro
JO.OuJ
.»C.OOP
7P.OO')
I
A
-------
COMPLETED ANALYSIS HEPORf
M
D8SPOSAI
RfPUft? OAir 90/07/11
PROJECT TIATJ
„ i ^^^mt v • mu » a *
' f ^P
~ DATE TIKE •.
STATION NO fROK Of OEPIH LABNfl PARMO PARA«ETFR NAS'.F.
- TO — "OAT " ' ' •"•
•• 5 7B 10 14114 ETHVlflENrENE
— •••• ' 34476 Hr.TIW.ENF. CHLORIDE
14471 MMHrt CHLORIDE
14290
34491
.... 14114
34309
"™" '."• " 144 f 4
344B3
34495
••• "•' ••"" ' 142m
_ 34? It
JOOHOIB734 ftO/06/li 0900 1101.0 57BII
0101?
01007
~ ~" ."."- 01012
01027
• •• ; •- — oioi«
01047
' "" "" " " *I90O
OIQ5I
~' : ' "0106?
0109?
01059
.. _ - _ 6109'*
0107?
1 oiool
01012
". ' OI02f
„ ..01014
71900
01051
0106?
" " "" ' ' '• 0109?
0114?
' - ' ' 01059
01092
J0000 11234 00/06/12 1519 1002.0 57BI1
. " "' 6l«7?
k ....... ... . . 01002
0102?
01034
01042
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70.0CJ
70.ore
70.0C»
70.00?
70. 0")
7^.0'-
70.000
70.
VST^
-------
I-
NO 129
MOJEC? NAM
FTON DISPOSAL
c t&EWMf OATi
MOJECT DATE
9MM/)t
•VR/OI'
STATION NO ' FROM OF OE'TM LABNO PAANO
...... Tn — -MV ••-
5?020 14110
,..-.- ^ 14504
14549
14564
" ."" . 141 14
1442*
... . ... . JMJ|
1441*
_ 14110
14114
" " 14104
144 ?0
, 1440J
1440?
14211
•— 142I«
" _ 010??
01012
0102?
01014
1 " '•" ~ ' ' " 0104*
?|900
* "" " " " " "~ ' 01051
010*?
0109?
0114?
01059
01092
PARAMETER NAME
CHLOROFORM
Itl-OICIN.OftOETMVlf'M:
|,2-IRANS DICMIOROCIMYLCN*
' 1,2-DlCllLOROPROf'ANF:
1 1 1-niCIHOROf RUf UFNE
ElHVLBtNlENE
I*ETMVLENF CHLORIDE
flETMVL CHLORIDE
HEIHU CROMIOE
OICHLQROMOMUPETHAfft
01 CMLUROniFLUOAOHE THANE
CMLORUDlflRUMUMEVtiAW ~ *
TETRACIILOMOE INUENE
TiiluiNE
IRICNtOROETNUENE
* VlNVL CMLbUlUt
ACROIEIN
ACRVLONITMU ~~ ' '
SILVER
RERVLLIUft .
CADMIUM ' ' " -
CHROMIUM
MERCURY
LEAD — •
1ICREL
4NIIMOMV
SriCNIIlM
(t
20.000 • '.T.
20.000 • * •:*
MOflO " ~ » ' "
20.000 • '
20.000 .
20.00C
20.000
20.000
20.000
20.000
20.000 "
20.000
2O.OOO .
20.000
20.000 '*~~
20.000 * _'
2o!ocr
2I.4C'%
|4.2fJ f
2ll900 *
29.100
ll.O'O
•* 20.000
20.000 v
f 20. 000 >A
/• 9.500
JOOOOI0214 tO/04/12 I2M H04.0 5?iJ2
J4624 2«4.4-f*ltMtIIC riUl
14700 ACENANITNENE
19121 BrNIIDENE
14554 I.2.4-TRICHLORORCN1ENE
1«»6|—MtiiCHibRJfcENIlNF
14199 HEHACHLOROETHANE
UG/RG
UG/RG
UG/RO
UG/RG
UC/RG
UC/RG
UC/RG
UG/RG
IM./RG
IK/RG
IN;/RG
UG/RG
UG/RG
UG/RG
~UG/RG
UC/RG
SEOIMENI
SEUINtHf
SEUINlNf
SEDIMENT
SEDIMENT
SEDIMENT
SEOINEN?
SfDIMFN?
SEDIMENT
SEDIHINT
SEDIMENT
SEDIMENT
SEUIMfNt
PEDIMENT
•sfOIMFNf
SEDIMENT
tf
U
U
U
U
U
U
U
U
U
U
U
U
U
ii
U
10.606
20.000
J0.000
20.000
10.000
20.000
10.000
20.000
20:090
20.000
20.000
20.000
20.000
0.0C
20.000
-------
^^ I
llCU -WOJICI NO B29 "•" ' ' " ~" " ~ "•••'"
: ^^
OAIE 7INE
1 SfATION NO , FROM OF OEFFN LABNO FARNO
1 ' 97022 1427*
14919
149*9
14974
" 14*14
14149
" 34179
14*44
" ~ ' " ' 14*.I9
342N*
147BI
14114
141B9
34411
34449
34490
' " " ' '"" ' ' " 34441
3443*
144i|
19IG2
" ' ' 34719
3*112
"'" ^ "' ' 34999
14119
14144
14979
' 34290
_ 34731
34121
14701
-. . •„ 14221
14924
1 / ) .,.,,„.,_. . ,.,. _„. 141R4
1 " ' " 144*4
,MI, ,..,.;._, , 14951
3440*
........ 34472
I4«7B
. ., OI07B
01061
. , 01011
OI02B
, ; . . 01029
010*1
71921
01092
. .... OIOAB
0109*
01I4H
~tOHPUfEO ANALYSIS HWOAf '
FROJCC? NAWE FRINCifON OISFPSAI
FARAffttER NANE
niSU-CMiOROCTHVLI fl.
2-CMlORONAFMrilAirNE
lt2-OICNlHROBF.NIENE
1 j4-t»|f. W.OROBI NItNF
1, 1* -0 ICNLOROHI!N£ IbENT
2*4-1. irtlfROrtHUCNF
2*»-fllHI IROKiLUEMC
l,2-UIFM»:»inMyUR4/IME _ _
4-CMtOROPMCNYl FHF^VL E7.
4-MUMUF1IENVL Plft'lVt Ef.
BISI2-Ct)HOROISUfRl)FVLI EfM
hlSI7-ClliUllH:iNftKVI MFIM.
Iff R ACNi DROOUIADI ENC
1 Stll*l«RII*(L
NAFMIIIALFNE
flllRtlBENIENE
N-NI IROSnolFHTNVLAf 1 IF
" N-Nl iNOSnOi-N-FRilFVLAHiHl
nisir-rrnvLHcivit PHHIAL.
HUIVL BFN2VL PM1MAIAIC
UI-N-HUIVLFF1IIHALAIE J
ni-N-nUVt PMlllALAtt " " i
_I»IEIIIU FHIIUIAIE !
1.2-HFN/ANIHRACFNE
refcin A PYRCNC
1 1 • 1 2-*tN!OFLUi*AMfHEilE
CKRVSFNT
rinwrw ..... . ,. .,,. , ,, ., ,.,
FiiENANrNKLNC
. 1*.? ,H <
•7.0000
.40000'.*
. 740000
.900000
. 700000
19.0000
IB.OOOO
.90QOOOF-OI
IO.OOOO
9.00000
.100000
.100000
U
U
U
U
U
U
U
to
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
If
ir
u
i'
C
u
"i«
, i"
is
i
i
t
L
t
K
R
R
R
J
R
! i ' •", 1"
SO OR OC ;,ft'i
•so »Atnr*r;
20.000 * tfl
20.000 i . •>• ; A«
20.000 -r •? *»•;'>!
20.000 *•*•'
20.000 -1 , *i!
20.000 * ' ..
20.000
20.000 '
20.000 *'
•"• 16.M5 . ' ,
20.000 w> ,
20.000 "f
20.000
20.000 : '—
20.000
20.400
20.000
20.000
20.000
20.000 '"
20.000 .
20.079 • :
20.000 !
20.000
20.000
70.000
20.003
20. oc:
20.000
70.-JOC •
70.00?
20.040
•* 20.000
" J6.doc :
', « 20.003 : .
f 20.00: , j
rt 20.090 ;; ' S
20.000 ,'•?' I
2.0.00"
20. or.
20.00-
23. OP-
20. Ot
?0.00
20.00 >
Jb.ooi
70.000
20.00U •
70.000
70.0-0
20.000
2 ft. 000
jflnQi)
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>
1
1
1
M
>
1
M
1
I
»
1
1
1
1
i
I
I
1
»
»
1
»
1
»
1
•
WV' " j^^"" " " " COMPUTED 2-fCTRAON.UROEfllAMf
. f... ...... ^.r..,.^ -~ ,-.-.. • M1|4 CHirmnfTHANC
34211 BISICIUOROMCTHUI Cf.
" " - J%fw j-iMUMHMETHU V|HVL ET.
, 34310 Ct%URUro*N
" 34994 t.i-Mtmrtnl^llViHV
34549 U2-IRANS DICNirmOCfllVlENE
" """" " " " ' 34344 lt7-OICHlOROPRUMHt
345*4 1.1-riCHlOROPRUPVLENE
1 34lt4 CtHvUENKNI
3442* NCIIIVLF.NE CHI OR If It
' 14421 METHVl CNLURIPf
_.. . . 144U ITTliyi MUH||>E
3*710 ItMIIMIVUHN
34330 UICHLUROHRUNUHC THANE
34491 r»ICIHnMOfLUOROmiMAMf i
34314 OICIIifMUOIFLUfWOnCTNAr«] |
3*309 CIHLORUniPRIIMUNEtMAl«E 1
3**VO fETRACIILOROETHVUNE 1
MC/RC
MC/RC
UC/RC
— UC/RC •
UC/RG
UC/RG
UC/RG
UC/RC
UC/RG
~~UC/RC
UC/RC
* UC/RC
UC/RG
UC/RC
UC/RG
i — vr./ftc~
UC/RG
uc/k«
UC/RG
UC/RO
UC/RG
— uc/«c"
UC/RG
UC/RG
UC/RG
UC/RG
UC/RG
"Ufc/RG
UC/RG
UC/RG
UC/RG
i'C/RG
I«/RG
' UC/RG
UC/RG
UC/RG
UT./RG
UV/RG
UC/RG
- UC/RG
UC/RG
UC/RG
UO/RC
UC/RG
UC/RG
"iih/iic"
UC/RC
UC/RG
UC/RG
I UC/RC
! UC/RG
UC/RC
I UC/RC
REPORT U
PROJECT
AIE
OAT
CHEMISTRY VAIUE C RENARR
SEOINCNT .200000 R
SEOINENf 3*.0000
SEOINENf U
'SEDIMCNf
SEOINENf
SEOINCNf
SEDIMENT
SEDINCNT
SEOINCNf
•»EO|N(M
SEOININf
SfOINCNf
SCOINCNf
SCDINCNf
SEOINENf
" StOINTM
SEOINCNT
SEOINENf
SEOINCNT
SFOINCNf '
SEOINCNT .-
SlOIHChf
SEOINENT
SEOINENf
SEDIMENT
SEOINENf
SCOINCNf
iloiNEiir " i.fCodd '
SEOINEIII
SEOINCNf 3*90000
SCDINCNf
SEOINCNf
SEDINFNf
• SEOINCNt
SEOINENf
SEOINCNf
SCOINCNT
SCtlNENf
SCOINfNf
"'SEDINCNt
SEOINCNf
SEOINENf
SEOINCNf
SEOINCNf ft 3.0000
SCOINENf
"SCOINENi
SEDINENf
SCOIMtMl
SEOINCrif
SFOINFNT
SCOIMFNT
SCOINCNf
SEOINENT
II
U
U
U
U
U
"IT
U
II
U
U
U
If
U
u
u
u
u
u
u
u
u
u
u
u
u
u
V
li
u
u
u
u
u
u
II
•1
u
-.1
•I
u
•J
•J
y
u
L
u
v jm
E BO/OT/O] .. i,4/i.:<
20.000 , .',. •*
20.000 ' .jj.
20.000 V.
20.000 ' *
' 10.AOO
20.000 ;.. *
20.000 ; ,
20.900 . .
70.000 * ~
20.000 * V
26.000 •
20.000
20.000 ~ ~
20.000 •»
20.000 '" .
20.000
10.000 •
70.000
20.00'
20.000
20.000 ~
20.000
70.000
2O.OOO
20.000 '
, 20.000
20.000 '"' '"'
t 20.000
* 20.000
tf 70.000
20.000
70.0CO
20.000
20.000
70.01N'
20.or :
70.0-.:.
20.0);
io.oof?
|0.0"»
70.011-
70.00U
70.0UU
20.000
20.000
70.00'.
70.0'M
70.00*
-------
5 :
MO J»Tr NO' 129 "—
• TO DAY
commit
: • wiurer MAM MINCCIH* DISPOSAL
»f«nii Mil to/offl!
sr*ricm NO
IABNO
5TI22 14481
I44ir
144«5 VltlVl CIH1MIOE
*Cluiim
ACMVlUNIfRIU
rnnjccf
CMCniSlftV VAtUF C
SO tM OC '
USD VAtlOf?~
IIC/K6 SEOINENf 14.0000 20.000 Vi ».'
IIC/KC SioiHfMf u jo.ooo " 7*^"••
UC/K6 SEOINCHT U 10.000 1- ;'.
ue/w • scbiMcNf -- u - io;ooa j '.
VC/KC 5foincur « .ao.ooo .J:. ,
I
I
I
I
I
,e>.
.......-i i .^.4 I_IXX'. {'.(I »> .» i I \ niriiii»
.' I, rl ( | | ( , I I' | )_!• ( | !MI Hi'
:. L.
r 'iii i !•* i ii • i < i •/ u i / n »
• '111 I !•* I li'll
I
/I
I
------- |