EPA/AA/CTAB/TA/83-5
Technical Report
Low Mileage Catalyst Evaluation
with a Metnanol-fueled Rabbit
- Interim Report
by
Robert D. Wagner
Larry C. Landman
May, 1983
NOTICE
Technical Reports do not necessarily represent final EPA
decisions or positions. They are intended to present tech-
nical analysis of issues using data which are currently
available. The purpose in tfhe release of such reports, is
to facilitate tne exchange of technical information and to
inform tne public of technical developments wnich may form
the basis for a final EPA decision, position or regulatory
action.
U. S. Environmental Protection Agency
Office of Air, Noise and Radiation
Office of Mooile Sources
Emission Control Technology Division
Control Technology Assessment and Characterization Branch
2565 Plymouth Road
Ann Arbor, Michigan 48105
-------
EPA/AA/CTAB/TA/83-5
Technical Report
Low Mileage Catalyst Evaluation
with a Methanol-fueled Rabbit
- Interim Report
by
Robert D. Wagner
Larry C. Landman
May, 1983
NOTICE
Technical Reports do not necessarily represent final EPA
decisions or positions. They are intended to present tech-
nical analysis of issues using data which are currently
available. The purpose in trhe release of such reports. is
to facilitate tne exchange of technical information and to
inform the public of technical developments which may form
the basis for a final EPA decision, position or regulatory
action.
U. S. Environmental Protection Agency
Office of Air, Noise and Radiation
Office of Mobile Sources
Emission Control Technology Division
Control Technology Assessment and Characterization Branch
2565 Plymouth Road
Ann Arbor, Michigan 48105
-------
-2-
Background
The use of pure methanol as an automotive fuel could allow the
use of less expensive exhaust catalysts. Two important bene-
fits are expected from the use of methanol compared to unleaded
gasoline. The benefits are reduced levels of catalyst poisons,
such as lead and sulfur, and reduced exhaust gas temperatures
at the catalyst inlet. Both major mechanisms of catalyst de-
activation, poisoning and thermal degradation, could be less
severe.
The purpose of this program is to evaluate various exhaust
catalysts at low mileage on a pure methanol-fueled Volkswagen
Rabbit. HC, CO, NOx and formaldehyde emissions will be
measured to identify which catalysts are the best candidates
for durability testing in a later program. Catalyst formula-
tions that are eventually selected for durability testing
should cost no more, and preferably less, than the original
catalyst on the vehicle.
All candidate catalysts should provide the capability to meet
the 0.41 HC and 3.4 CO levels at low mileage with substantial
margins of safety. Additionally-, 3-way catalysts should pro-
vide emissions well below the 1.0 NOx level.
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-3-
Conclusions
1. Several catalysts have been identified as good candidates
for vehicle durability testing. All of these catalysts
contain noble metals. The catalysts recommended for dura-
bility are 1) platinum and rhodium in a ratio of 5:1 at a
loading of 40 grams/cubic foot (a loading identical to the
original catalyst on the vehicle and identical to that used
on the forty vehicles provided to the California Energy
Commission), 2) platinum and palladium in a ratio of 3:2
at 20 grams/cubic foot, and 3) all palladium at a loading
of 40 grams/cubic foot. All catalyst volumes would be 75
cubic inches. All catalyst substrates would be 400 cells
per square inch with a wall thickness of 6 mils.
2. One catalyst was tested which was all base metal. It was
pure copper mesh. The copper mesh provided some HC con-
version over the highway cycle, but not much else. CO
control over the FTP was poor with the catalyst, and it
provided little NOx control with stoichiometric exhaust
conditions.
3. One catalyst has been tested which includes substantial
amounts of both base and noble metals. The inclusion of
the base metals provided no significant emissions benefit
in comparison to other palladium catalysts in this study.
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-4-
Future Effort
The results which nave been obtained so far will be provided to
the vehicle and catalyst manufacturers who have assisted us in
tnis program. We will request their advice on the following
subjects.
o how to improve tne emissions control capability of prev-
iously tested and poorly performing catalysts,
o which additional catalysts should be tested at low mileage,
o how to further reduce the cost of durability-candidate
catalysts, and
o now to improve tne durability emissions performance of
those catalysts which performed well in our low mileage
testing.
We now plan to further evaluate the copper mesh after an acid
dip and with the addition of insulation to the exhaust system.
The silver catalyst will be further evaluated with exhaust
system insulation and possibly with some varying thermal pre-
treatments. A copper oxide catalyst will also be tested.
Based on our testing to date, it appears as though we may need
to retain rhoaium for acnieving tne lowest possible aldehyde
levels. New catalyst candidates could include more lightly
loaded platinum/rnodium catalysts in the 10-20 gram/cubic, foot
range and palladium/rnodium units in the same loading range and
with Pd: Rh ratios of 5:1 or 10:1.
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-5-
Test Vehicle Description
The test vehicle is a 1981 model year Volkswagen Rabbit. It
was modified by Volkswagen to operate on methanol plus 5.5%
isopentane. It is a 4-door sedan equipped with air condition-
ing/ a 3-speed automatic transmission/ and a 1.6 liter engine.
The compression ratio of the engine is 12.5:1. Maximum power
output is 88 horsepower at 5600 RPM (1)*. The tire size is 155
SR 13. The tires are Michelin XZX radials. It was tested at
2250 pounds inertia weight and 7.3 actual dynamometer horse-
power.
The emission control system/ as equipped by Volkswagen includes
feedback controlled/ continuous fuel injection (K-Jetronic) and
a three-way catalyst. The catalyst provided by VW was 4.0
inches in diameter and 6.0 inches long. It contained platinum
(Pt) and rhodium (Rh) in a ratio of 5:1 at a loading of 40
g/ft . The vehicle is described in more detail in Appendix
1, which was taken from a Volkswagen emission control status
report (2) to EPA.
The emission control system was modified oy EPA to include a
pump-type air injection system. The air was injected into the
exhaust at a location about a foot downstream from the oxygen
sensor. A manually adjustable valve was installed in the line
between tne diverter valve and the exhaust inlet. This valve
allowed us to vary oxygen concentration into the catalyst while
operating the engine in the closed loop mode.
*Numbers in parenthesis are references listed at the enc9
this report.
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-6-
Test Sequence, Instrumentation, and Fuel
The initial plan included testing of the vehicle and each
catalyst over the following sequence:
1975 Federal Test Procedure
Highway Test Procedure
20 mph steady state
30 mph steady state
40 mph steady state.
The sequence would be repeated twice for each catalyst at each
of three exhaust oxygen levels. The higher two of the three
exhaust oxygen levels were measured at the catalyst inlet using
a Sun oxygen analyzer -and were obtained at 30 miles per hour
steady state. The three oxygen levels were stoichiometry (or
near 0%), 3%, and 5%. By testing at different exhaust oxygen
levels, we could evaluate each catalyst as a 3-way and also as
an oxidizing catalyst.
AS the project proceeded, idle and a 10 mph steady state were
added to the sequence and the 40 mph steady state was deleted.
HC, CO, NOx, MPG, methanol, methane, and aldehydes were ini-
tially measured over each test in the sequence. Aldehydes were
deleted during steady states in more recent testing. Methanol
was deleted for all testing as the program progressed.
Exhaust HC emissions, as reported here, were measured with a
flame ionization detector (FID) from Beckman (model 400) . No
corrections in the results were made for either the FID re-
sponse to methanol or the difference in HC composition with
methanol as the fuel. NOx emissions were measured with a
chemiluminescent NO/NOx analyzer from Beckman (model 951A). CO
-------
-7-
9
was measured with infrared analyzers from MSA and Bendix.
Methane was measured with a gas chromatograph (Bendix 8205
methane analyzer) . Aldehydes were measured by high pressure
liquid chroraatography (HPLC). See Appendix 2 for more
details. Gaseous methanol was measured by a gas chromatograph
(Perkins-Elmer model 3920) .
The test fuel which has been used is pure methanol. Three
batches of the fuel have been used, and one has been analyzed.
The fuel analysis is presented in Appendix 3.
FTP Test Results
The Rabbit has been tested with a total of nine different cata-
lysts. Those catalysts are described in Table 1. Also, the
vehicle has been periodically tested with no catalyst to assure
that major changes in emissions without a catalyst have not
occurred over the duration of the test program. The vehicle
emissions with no catalyst as a function vehicle odometer
reading are shown in Figures 1 and 2. There was an oxygen
sensor change to the emission control system which may have
resulted in a slight shift in FTP emissions at about 6,300
miles; however, HC, CO, NOx, and methanol emissions have been
reasonably stable over the test program to date.
Aldehyde emissions were not as stable as desired. The cause of
variablity in the aldehyde emissions is being investigated. We
know the column was changed in the liquid chromatograph (to a
nominally identical column) just prior to generating the value
of about 130 mg/mi in Figure 2. The impact of the column
change on the variability is unknown. It is possible that the
aldehyde emissions are of such a small magnitude that we may
not be able to get rid of the variability with this particular
vehicle and test equipment.
-------
-8-
Table 1
Catalysts Tested to Date
Abbreviated
Catalyst
Code
5 Pt: Rh(40)
12 ?t: Rh(40)
12 Pt: Rh(40)*
3 Pt: 2 Pd(20)
CPSI
and
twall
[I/in2]
[mils]
300,10.5
400,6
400,6
400,6
Substrate
Size
[Diameter
and
Length]
4.0" x 6.0"L
4.0" x 6.0"L
3.18" x 6.68"
x 6.0"L
4.0" x 6.0"L
Substrate
Volume
[in3]
75
75
110
75
Noble
Metals
Ratio Load
[g/ft3]
5Pt:lRh 40
12Pt:lRh 40
12Pt:lRh 40
3Pt:2Pd 20
Major
Base
Metals
Pd (40)
400,6 4.0" x 6.0"L 75
Pd
40
Pd + BM (35) 400,6 4.0" x 6.0"L 75
Pd
35 Proprietary
transition
elements
Cu
N/A
4.25" x 12.0"L 170
None
Copper mesh
7.7% packing
density
Pd (20)
Ag (150)
400,6 4.0" x 6.0"L 75 Pd
400,6 4.0" x 6.0"L 75 Ag
20
150
*This catalyst is a "racetrack" in cross section. All other catalysts are circu-
lar in cross section.
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10
8-
a
6-
O
2-
FIGURE 1
EMISSIONS WITHOUT CATALYST
0% 02
•Ar-
Legend
0 HC
A CO
X NOX
3000 4000
5000 6000 7000
ODOMETER MILES
8000
-------
350
300 H
g 250-
CO
s
200
150-
100
FIGURE 2
ALDEHYDES WITHOUT CATALYST
0% 02
3000 3500 4000 4500 5000 5500 6000 6500 7000 7500
ODOMETER MILES
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• -11-
In Table I, the catalysts have been referred to by an an Ab-
breviated Catalyst Code. The original catalyst on the vehicle
contained platinum and rhodium in 5:1 ratio at a loading of 40
grains per cubic foot of substrate volume. As an example of the
Abbreviated Catalyst Code, this catalyst has been referred to
as catalyst 5 Pt: Rh (40) .
All catalysts in the group are of identical volume except for
the 12 Pt:Rh (40)* catalyst and the Cu catalyst. The 12 Pt: Rh
(40)* catalyst is a sample of 110 in . Initially we planned
to test all samples in two volumes; however/ the smaller noble
metal samples were so active that increased catalyst volume
would likely be able to provide little improvement in low
mileage conversion efficiency. If durability testing is un-
successful/ then larger catalyst volumes may be one of several
possible paths to take.
All catalysts used in the program were zero mile catalysts ex-
cept for the original catalyst on the vehicle. Assuming this
catalyst had been on the vehicle since manufacture/ it had ac-
cumulated less than 3/000 miles prior to testing at EPA.
Tailpipe emissions from this vehicle with no catalyst at stoi-
chiometric operating conditions averaged 0.92 HC, 7.52 CO/ 2.08
NOx. In comparison to gasoline-fueled vehicles, these simul-
taneous CO and NOx levels are low for an engine operating at
stoichiometry with no EGR.
-------
-12-
Taoles 2, 3, ana 4 present summaries of the FTP results which
were obtained at each exhaust oxygen level. Non-methane HC
results are nearly identical to total HC results at all three
oxygen levels with and without catalysts. This indicates that
there is virtually no methane in the exhaust. Average HC and
CO emssions are below levels of 0.2 HC, 2.0 CO for all except
the silver (Ag) , copper (Cu) , and mixed metal (Pd + BM) cata-
lysts at all oxygen levels.
Individual emission test results are presented in Appendix 4.
Additional statistics, including standard deviations that cor-
respond to the the mean values in Tables 2, 3, and 4 are shown
in Appendix 5. A listing of unscheduled vehicle maintenance is
provided in Appendix 6.
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Table 2
Summary of the FfP Test Results with
Operation as 3-Way Catalysts
Catalyst
None
5 Pt: Kh (40)
12 Pt: Kh (40)
12 Pt: Kh (40)*
3 Pt: 2 Pd (20)
Pd (40)
Pd + BM (35)
Cu
Pd (20)
Ag (150)
Oxygen
Level
0
0
0
0
0
0
0
0
0
0
HC
.92
.15
.11
.13
.15
.17
.28
.90
.18
.54
NMHC
.91
.14***
.11***
.14**
.15***
.15***
.27
.90
.18
.53
Methanol
ly/iiii /
2.18
.21
.33***
.82**
N/A
.35***
N/A
N/A
N/A
N/A
CO
7.52
.78
.69
.77
1.47
1.99
2.85
7.52
1.84
6.53
NOx
2.08
.84
.62
.76
.85
.74
1.97
1.88
.67
2.03
Aldehydes
(rag/mi)
241.6
20.3
11.6
11.4
29.5**
41.5
118.8
291.9
41.0
55.4****
Number
MPG of
Tests
13.89
14.18
13.97
13.95
13.78
13.47
14.14**
13.69
13.81
13.85
Up to 14
Up to 6
3
2
3
i
3 C
2
2
3
4
N/A means data are not available
*Kacetrack, others are round
**based on 1 test
***based on 2 tests
****based on 3 tests
-------
Table 3
Summary of the PI'P Test Results with
Operation as Oxidizing Catalysts
Catalyst
None
5 Pt: Kh (40)
12 Pt: Rh (40)
12 Pt: Kh (40)*
3 Pt: 2 Pd (20)
Pd (40)
Pd •*• BM (35)
Cu
Pd (20)
Ag (150)
Oxygen
Level
3
3
3
3
3
3
3
3
3
3
HC
.92
.14
.12
.13
.16
.14
.28
.90
.15
.43
NMHC Methanol
.81****
.14
.11
.12
.15
.14
.27
.90
.15
.46***
vy/nu./
2.08
.59
.31
N/A
.28
N/A
N/A
N/A
N/A
N/A
CO
7.26
.60
.39
.40
.35
.38
2.05
7.29
.40
5.93
NOx
2.09
1.95
2.01
2.05
2.07
1.98
1.95
1.82
1.90
1.99
Aldehydes
(mg/mi)
264.3
15.4
15.6
14.4
72.9**
68.0
129.4
322.3
94.2
N/A
Number
MPG of
Tests
13.93
13.75
14.01
13.74
13.43
13.43
13.90**
13.44
13.83
13.71
Up to 5
1
3
3
i
2 £
i
2
2
2
2
3
N/A means data are not available
*tocetrack,. others are round
**based on 1 test
***based on 2 tests
****based on 3 tests
-------
Table 4
Summary of the FTP Results with
Operation as Oxidizing Catalysts
Catalyst
None
5 Pt: Kh (40)
12 Pt: Kh (40)
12 Pt: Kh (40)*
3 Pt: 2 Pd (20)
Pd (40)
Pd + hM (35)
Cu
Pd (20)
Ag (150)
Oxygen
Level
(%)
5
5
5
5
5
5
5
5
5
5
HC
.90
N/A
.12
.13
.19
.16
.37
.87
.13
.54
NMHC
.97***
N/A
.12
.13
.19**
.15
.36
.86
N/A
.53
Methanol
tg/mi)
2.46
N/A
.32
N/A
.36
N/A
N/A
N/A
N/A
N/A
CO
7.51
N/A
.40
.46
.40
.36
3.66
6.93
1.31
6.96
NOx I
2.09
N/A
2.10***
2.09
2.03
2.05
1.94
1.82
1.91
1.89
VIdehydes
(mg/mi)
194.2
N/A
21.0
20.8
117.4
141.9
279.5
313.9
104.0
N/A
Nuntoer
MPG of
Tests
13.83
N/A
13.91
13.76
13.51
13.26
13.85
13.47
13.70
13.79
Up to 6
0
4
1
2
3
3
2
2
1
N/A means data are not available
*Kacetrack, others are round
**based on 1 test
***based on 2 tests
en
-------
-16-
Average raethanol emissions ranged from 0.21 to 0.82 gram per
mile at stoichiometric exhaust conditions and with catalysts.
At tne 3 percent and 5 percent oxygen levels, methanol emis-
sions with the catalysts ranged from 0.28 to 0.59 gram per mile.
The catalysts which contain rhodium were expected to have sig-
nificant NOx activity when operated as 3-way catalysts. The
other noble metal catalysts also had good NOx activity in these
low mileage tests. Based on the performance of vehicles fueled
with gasoline, this activity may not be retained over substan-
tial mileage accumulation with the catalysts not having rhod-
ium. As expected, none of the catalysts provided NOx activity
under oxidizing exhaust conditions.
Aldehyde emissions were handled much like HC emissions by the
catalysts. All the noble metal catalysts showed reductions in
aldehydes. Aldehyde levels generally increased as exhaust oxy-
gen level increased.
Catalyst efficiencies were calculated for eacn catalyst at each
exhaust oxygen level. The results of these calculations are
presented in Tables 5, 6, and 7. Catalyst efficiency as used
here is defined as tailpipe emissions with no catalyst minus
tailpipe emissions with a catalyst, the difference divided by
tailpipe emissions with no catalyst.
HC efficiencies are greater than or equal to 79% for the noble
metal catalysts, except silver, at all exhaust oxygen con-
ditions. CO efficiencies exceed 73 percent for all noble metal
catalysts, except silver, at all oxygen conditons. The lowest
NOx efficiency for these catalysts (again excluding silver) is
59 percent at stoichometry. No NOx efficiency is
-------
-17-
Table 5
CATALYST EFFICIENCY (%)
Oxygen Leve
Catalyst
5 Pt: Rh (40)
12 Pt: Rh (40)
12 Pt: Rh (40)*
3 Pt: 2 Pd (20)
Pd (40)
Pd + BM (35)
Cu
Pd (20)
Ag (150)
HC
83
88
86
83
82
70
2
80
41
CO
90
91
90
80
74
62
0
76
13
1 at 0%
2ff icienc
NOx
60
70
63
59
64
5
10
68
2
Methanol
91
85
62
N/A
84
N/A
N/A
N/A
N/A
Formaldehyde
92
95
95
86
83
51
-21
83
77
N/A means data are not available
*Racetracl<, otners are round
-------
-18-
Table 6
CATALYST EFFICIENCY (%)
Oxygen Leve
Catalyst
5 Pt: Rh (40) '
12
12
3
Pd
Pd
Cu
Pd
Ag
Pt: Rh (40)
Pt: Rh (40)*
Pt: 2 Pd (20)
(40)
+ BM (35)
(20)
(150)
HC
84
87
86
83
84
70
2
83
53
CO
92
95
94
95
95
72
-1
94
18
1 at 3%
Sfficiency i
NOx ^
7
4
2
1
5
7
13
9
5
lethanol
72
85
N/A
87
N/A
N/A
N/A
N/A
N/A
Formaldehyde
94
94
95
72
74
51
-22
64
N/A
N/A means data are not available
*Racetrack, others are round
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-19-
Table 7
CATALYST EFFICIENCY (%)
Oxygen LeveJ
Catalyst
5 Pt: Rh (40)
12
12
3
Pd
Pd
Cu
Pd
Ag
Pt: Rh (40)
Pt: Rh (40)*
Pt: 2 Pd (20)
(40)
+ BM (35)
(20)
(150)
HC
N/A
86
85
79
82
59
4
85
40
CO
N/A
95
94
95
95
51
8
96
7
L at 5%
fficiency f
NOx fr
N/A
0
0
3
2
7
13
9
9
iethanol
N/A
87
N/A
85
N/A
N/A
N/A
N/A
N/A
Formaldehyde
N/A
89
89
40
27
-44
-62
46
N/A
N/A means data are not available
*Racetrack, others are round
-------
-20-
achieved during oxidizing conditions. Aldehyde efficiencies
decrease as oxygen level increases. Aldehyde efficiency ex-
ceeds 64 percent up to 3 percent oxygen. If rhodium is used in
the catalyst, aldehyde efficiency is 89% or higher at all oxy-
gen levels.
The Cu catalyst has little impact on any FTP emission. The
silver catalyst has 77 percent aldehyde efficiency at 0 percent
oxygen and has modest HC efficiencies.
The palladium plus base metal (Pd + BM) catalyst does not ex-
hibit tne NOx efficiency of other Pd catalysts. Also, the HC
and CO efficiencies are poorer than for otner catalysts which
contain Pd. Apparently the amount of palladium present was not
utilized as well in this catalyst as in the others.
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-21-
Evaporative Emissions
A series of SHED tests measuring evaporative emissions were
performed in order to determine the effectiveness of activated
charcoal canisters in controlling the evaporative emissions of
methanol. The results of those tests are summarized in Table 8.
The first six SHED tests, performed on the car equipped with
its stock canister, results in average evaporative emissions of
1.74 grams per test. In order to determine the effectiveness
of the canister system, two additional SHED tests were per-
formed with the canister vent lines disconnected and vented to
the atmosphere. The results of those two tests averaged 1.73
grams per test. Those results seemed to indicate that the
original canister was not (at that time) effective in control-
ling evaporative emissions. Since that lack of effectiveness
might have resulted from the canister being saturated, ad-
ditional testing was performed with the car equipped with new
canisters. These tests also yielded results which were of the
same order of magnitude. Thus, it appears that the activated
charcoal canisters used in these tests are ineffective in con-
trolling evaporative emissions from this methanol-fueled
vehicle.
The flame ionization detector (FID) measurements in Table 8
were "corrected" to reflect the assumption that all the HC
detected was in the form of methanol (CH.,OH) , having a
molecular weight of 32.04243. No attempt was made to further
"correct" the table values to account for the fact not all the
methanol is being measured by the FID. The relative response
of the FID to methanol as compared to propane (the hydrocarbon
commonly used to calibrate the FID response) has been found to
range from 0.73 to 0.85 (3, 4, 5, 6).
-------
Test
Number
814597
814678
814677
815125
815163
815208
Test
Date
07-08-82
07-09-82
07-13-82
07-30-82
08-03-82
08-04-82
-22-
Table 8
Evaporative Emissions*
grams per test
Heat
Build
1.0046
0.6759
0.6618
0.8749
0.6897
0.6708
Hot
Soak
1.1030
1.0740
0.3795
1.4208
1.0062
0.8638
Total
2.1076
1.7499
1.0413
2.2957
1.6959
1.5346
Comments
Stock canister (#1)
816706 10-27-82 0.7096 0.9141 1.6237 Canister vent lines
816731 10-28-82 1.0334 0.8125 1.8459 disconnected
817499 01-20-83 0.7571 0.7447 1.5018 New canister (#2)
818980 03-25-83 0.8120 0.8512 1.6632 Canister #1 reattached
818982 03-29-83 0.7250 1.0663 1.7913 New canister (13)
818984 03-30-83 017674 0.9322 1.6997 Canister <*2 reattached
818986 03-31-83 0.8133 0.8961 1.7094
818988 04-05-83 0.6585 0.7783 1.4368
818994 04-08-33 0.7167 0.9193 1.6360 Canister vent lines
disconnected
* FID data "corrected" by assuming all hydrocarbons detected
were methanol, having a molecular weight of 32.04243.
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-23-
Highway Cycle Emissions
The noble metal catalystsf with the exception of silver, pro-
vide excellent HC and CO emissions over the highway test as
shown in Tables 9, 10, and 11. HC emissions are .010 g/mi or
less under all oxygen conditions. CO emissions are also very
low at 0.33 or less. As on the FTP, NOx is substantially re-
duced by the noble metal catalysts, except silver, during stoi-
chioraetric exhaust conditions.
The mixed metal catalyst performed well on the highway test.
HC and CO were highest at stoichiometry where they were .016
and 1.48 g/mi respectively. Some NOx reduction was also seen.
The copper catalyst showed some HC activity over the highway
test. The HC activity increased as the exhaust oxygen level
increased. CO, aldehydes, and NOx emissions were not strongly
impacted oy the copper catalyst. The silver catalyst has sub-
stantial HC and modest CO activity. Aldehyde emissions were
only measured at stoichiometry, and they were very low (less
than 3 mg/rai).
The copper and silver units have shown improved emission con-
trol capabilities over, the highway cycle as compared to the
FTP. Apparently the lack of a cold start and/or the higher
catalyst inlet temperatures are permitting the catalysts to be
more active. Additional efforts could be expended on these
catalysts to further increase catalyst inlet temperature during
all driving modes by insulation of the exhaust system.
Exhaust emissions over various steady state conditions were
also measured in our testing. These results, from idle to 30
mph, are summarized in Appendix 7.
-------
Table 9
Summary of the Highway Test Results with
Operation as 3-Way Catalysts
Catalyst
None
5 ft: Kh (40)
12 Ft: Kh (40)
12 Ft: Kh (40)*
3 Ft: 2 Fd (20)
Fd (40)
Fd + BM (35)
Cu
Fd (20)
Ay (150)
Oxyyen
Level
0
0
0
0
0
0
0
0
0
0
tic
.428
.002
.003
.008
.007
.006
.016
.304
.009
.024
NMIKJ Methanol
V
.419
.001****
.003
.009***
.007***
.005***
.012
.298
.007
.019
y/iiuj
.693
.004
.009***
.034***
N/A
.016***
N/A .
N/A
N/A
N/A
CO
6.67
.11
.05
.06
.22
.33
1.48
6.91
.38
4.26
NOx
2.81
.09
.61
.55
.64
.51
1.63
2.41
.35
2.74
Aldehydes
(mg/mi)
168.3
.2
.5
1.2
.9**
.7
3.1***
130.7
1.9***
2.4
MPG
17.20
18.08
17.32
17.72
17.16
16.98
17.59
17.03
17.26
17.10
Number
of
Tests
Up to 14
4
3
3
3 i
to
3 '
2
2
3
3
N/A means data are not available
*Kacetrack/ others are round
**based on 1 test
***based on 2 tests
****based on 3 tests
-------
Table 10
Summary of the Highway Test Results with
Operation as Oxidizing Catalysts
Catalyst
None
5 Pt: i
-------
Table 11
Summary of the Highway Test Results with
Operation as Oxidizing Catalysts
Catalyst
None
5 Pt: Kh (40)
12 Pt: Kh (40)
12 Pt: Kh (40)*
3 Pt: 2 Pd (20)
Pd (40)
Pd + BM (35)
Cu
Pd (20)
Ay (150)
Oxygen
Level
/U k
(*)
5
5
5
5
5
5
5
5
5
5
tic
.398
N/A
.010
.010
.010
.009
.014
.150
.009
.023
NMHC
.431***
N/A
.007
.008
.006
.006
.009
.144
.005**
.018
Methanol
/ / -I V
(g/mi)
0.87
N/A
.006
.027
.009
N/A
N/A
N/A
N/A
N/A
CO
6.30
N/A
.002
.028
.004
.013
.417
6.18
.003
5.07
NOx
2.84
N/A
2.78****
2.80
2.78
2.72
2.64
2.21
2.61
2.42
Aldehydes
/ / •• \
(mg/mi)
141.7
N/A
1.9
2.2
3.0
2.7
14.5
124.2
2.9
N/A
MPG
17.30
N/A
17.39
17.37
17.05
17.01
17.70
16.73
17.03
18.20
Number
of
1V*cft-c
J.6SCS
Up to 6
0
4
1
2
2
2
2
3
2
i
to
cr>
1
N/A means data are not available
*Kacetrack, others are round
**based on 1 test
***based on 2 tests
****based on 3 tests
-------
-27-
Cost and Efficiency per Dollar Estimates
An estimate of the sticker cost of each catalyst in this study
has been generated using the methods of reference 7. Sticker
cost means the cost to the consumer of the catalyst as it is
reflected on the sticker of a new automobile at an automobile
dealership. The information in reference 7 has been updated
1) to use 77 percent of the current producer prices for noble
metals as stated in the May 13, 1983 edition of American Metal
Market - Metalworking News Edition and 2) to account for in-
flation between 1977 and 1983 at an estimated rate of ten per-
cent per year. We use 77 percent of producer price for noble
metals to account for what we estimate are the discounts to the
automobile manufacturers due to high volume, long term pur-
chases.
Each catalyst has been evaluated as an oxidizing and 3-way
catalyst on an "efficiency per dollar" basis. This means that
for an oxidizing catalyst, the previously calculated catalyst
efficiencies for HC, CO, and aldehydes were summed and then the
total was divided by the estimated sticker cost. The only dif-
ference in the calculation for 3-way catalysts is that catalyst
efficiency for NOx is added to the HC, CO, and aldehyde ef-
ficiencies.
The results of these calculations are presented in Table 12.
The estimated sticker costs of the catalysts in our program
range from $58 to $150. The costs shown in Table 12 indicate
more accuracy in our cost estimates than we would like to con-
vey to the reader. Normally we would round these costs off to
the nearest 5 or 10 dollars. In this case, rounding to the
nearest 5 dollars would mask real cost differences in the
catalysts and would make non-identical catalysts appear to cost
the same amount.
-------
-28-
Table 12
Sticker Cost and Effici
Dollar of Each Cat«
vJ 1* X W *\ C *•
Catalyst Cost
($)
5 Pt: Rh (40)
12 Pt: Rh (40)
12 Pt: Rh (40) *
3 Pt: 2 Pd (20)
Pd (40)
Pd + BM (35)
Cu
Pd (20)
Ag (150)
Canned substrate
only/ no catalyst
111
110
150
75
72
70**
58
64
65
56
0% Oxygen
2.92
3.13
2.23
4.12
4.20
2.69
-0.16
4.79
2.06
N/A
Lency per
ilyst
Lency Per DolJ
3% Oxygen
2.44
2.51
1.83
3.33
3.52
-2.75
-0.36
3.78
1.10
N/A
'a •• -i ^ __
5% Oxygen
N/A
2.46
1.79
2.84
2.84
0.96
-0.86
3.55
0.73
N/A
* Racetrack others are round
**Does not include the cost of base metals.
-------
-29-
Strictly on the basis of the efficiency per dollar calcula-
tions, durability selection for 3-way catalysts would be made
in the following order of decreasing interest:
Pd (20),
Pd (40),
3 Pt: 2 Pd (20),
12 Pt: Rh (40) ,
5 Pt: Rh (40),
Pd + BM (35) ,
12 Pt: Rh (40)*,
Ag (150), and
Cu.
Additional consideration must be included, however, in the
selection of durability candidates. First, we must consider
that virtually all 3-way catalysts used for gasoline-fueled
vehicles contain rhodium. This indicates that rhodium is
likely needed for adequate emissions durability. The second
consideration is that durability testing is so costly that we
may want to test samples with the highest probability of suc-
cess, not the samples with least cost. With these considera-
tions our first priority samples for durability evaluation as
3-way catalysts are in decreasing order of importance:
5 Pt: Rh (40),
Pd (40) , and
3 Pt: 2 Pd (20).
Durability testing with other samples is not recommended. The
samples designated Cu, Ag (150), 12 Pt: Rh (40)*, and Pd + BM
-------
-30-
were oraittei on the basis of low efficiency per dollar. The Pd
(20) unit was omitted because it is like the Pd (40) catalyst
in all respects except that it contains only half as much pal-
ladium.
For durability operation as oxidizing catalysts, efficiency per
dollar would dictate selections in this order:
at 3% Oxygen at 5 % Oxygen
Pd (20) , Pd (20) ,
Pd (40) , Pd (40) ,
3 Pt: 2 Pd (20), 3 Pt: 2 Pd (20),
Pd + BM (35), 12 Pt: Rh (40),
12 Pt:Rh (40),
5 Pt: Rh (40), 12 Pt: Rh (40)*,
12 Pt: Rh (40)*, Pd + BM (35),
Ag (150), and Ag (150), and
Cu. Cu.
The selections at 3 percent and 5 percent oxygen are in nearly
the same order. Except for the Pd + BM catalyst and one less
catalyst to evaluate at 5% oxygen, the order is exactly the
same.
Since rhodium content has not been of importance in oxidizing
catalyst durability with gasoline-fueled vehicles, our recom-
mendations for durability evaluation of oxidizing catalysts
follow the efficiency per dollar calculations more closely.
For durability testing as oxidizing catalysts we recommend that
the following catalysts be considered as the highest priority
samples:
Pd (40) , and
3 Pt: 2 Pd (20).
-------
-31-
Again the final four samples on the basis of efficiency per
dollar were deleted from consideration. The Pd (20) sample
again was deleted since it is identical to the Pd (40) sample
except that it only has half as much palladium. Durability
emissions in theory should be somewhat lower with the Pd (40)
catalyst. The Pd + BM sample was not included since it consis-
tently performed at lower efficiencies than the Pd (20) and Pd
(40) catalysts.
-------
-32-
Summary
Over the FTP:
o Almost no methane is measured in the exhaust.
o Excellent HC and CO control (less than 0.2 and 2.0 grams
per mile, respectively) is achieved with all the noble
metal catalysts, except silver, at all exhaust oxygen
levels.
o All the noble metal catalysts, except silver, achieve NOx
levels below 1.0 gram per mile at stoichiometry.
o The addition of case metals -to a Pd catalyst did not im-
prove the catalyst.
o CO and NOx control are both poor with the base metal cata-
lyst.
Over tne highway cycle:
o Exhaust emissions are generally much less than on the FTP
on a gram per mile basis, except for NOx emissions. Ex-
cluding emissions with the copper catalyst (which is the
least active of all catalysts) and CO emissions with the
silver catalyst, little HC, CO, or aldehyde is emitted.
Based on cost, catalyst efficiency, and other considerations,
several catalysts have been identified which merit durability
testing as 3-way and as oxidizing catalysts. Additional cata-
lysts will be evaluated and additional effort will be expended
to improve emissions from catalysts which have performed poorly
to date.
-------
-33-
References
1. H. Menrad, G. Decker, and K. Weidmann, "Alcohol Fuel Vehi-
cles of Volkswagen", SAE Paper No. 820968, August, 1982, pp
9-12.
2. Status Report of Volkswagenwerk AG Audi, NSU Auto Union AG
and Volkswagen of America, Inc., submitted to the Environ-
mental Protection Agency, May, 1981, Volume 1, Section VII.
3. D.L. Hilden and F.B. Parks, "A Single-Cylinder Engine Study
of Methanol Fuel - Emphasis on Organic Emissions," SAE
Paper No. 760378.
4. R. Bechtold and J.B. Pullman, "Driving Cycle Economy, Emis-
sions, and Photochemical Reactivity Using Alcohol Fuels and
Gasoline," SAE Paper No. 800260.
5. H. Menrad, W. Lee, and W. Bernhardt, "Development of a Pure
Methanol Fuel Car," SAE Paper No. 770790.
6. G.D. Ebersole and F.S. Manning, "Engine Performance and Ex-
naust Emissions: Metnanol Versus Isooctane," SAE Paper No.
720692.
7. L.H. Lindgren, Cost Estimations for Emission Control
Related Components/Systems and Cost Metnodology Descrip-
tion, EPA-460/3-78-002, March, 1978, pp 131-134 and pp
147-149.
-------
APPENDIX 1
Vehicle Description
-------
1-1
III. RESULTS
A. VRHTrTF. DESCRIPTION
1981 Volkswagen Rabbit "L" 4-Door Sedan - Model 177243
Vlf 1VWF80175BV012728 Engr. Car I 1285
Automatic transmission, air conditioning, 155 80R13 tires, radio and cloth
interior. (A vehicle with Vinyl "leatherette" interior was not available at time
prototype was built. This may have a small influence on evaporative losses, but
this will be negligible once the "new car" background level deteriorates.)
B. DETAILED COMPARISON OF PRODUCTION vs. METHANQL POWERTRAIN AND FUEL SYSTEM
ITEM
1980 PRODUCTION
METHANQb VEHICLE
Basic Engine
o Type
o Displacement
o Bore
o Stroke
o Compression Ratio
o Valvetrain
o Hated Power
o Rated Torque
o Other
- 827
- 1.6 liter (1588cc)
- 3.13 inches
- 3.15 inches
- 8.2:1
- Overhead camshaft
- 76 HP SAE net @ 5500 RPM
- 82.7 Ft. Ibs. SAE net
@ 3200 RPM
Fuel System - Bosch CIS Fuel Injection with
Lambda feedback control.
- 827
- 1.6 liter (1588cc)
- 3.13 inches
- 3.15 inches
- 12.5:1 (new pistons)
- Overhead camshaft
- Not measured
- Not measured
- GTI basic engine -
European high
performance engine to
withstand higher loads
- U.S. cylinder head.
- Same as Production with
calibration for Methanol
operation.
(Narrative description and schematic of system in Appendix I)
-------
1-2
nai
Fuel System (Continued)
o Fuel Pump
Pump Life
Other
o Accumulator
Maximum holding
pressure
o Fuel Filter
1980 PRODUCTION
METHANOL VEHICLE
o Fuel Distributor
System pressure
Calibration
Other
o Air sensor
o Fuel Injectors
- Life of Vehicle
- 2.5 Bar
4.6 - 4.8 bar
Optimized for gasoline
o Cold Start Injector
Quantity
Function
One
On for start only.
6 months to 1 year due
to corrosiveness of
Methanol.
Improved insulation on
wiring exposed to fuel.
3.0 bar (due to fuel
difference).
Bonding glue changed
for fuel compatability.
One way check valve
deleted (Incompatable
with fuel).
5.0 - 5.3 bar
Optimized for Methanol.
Material changes for
fuel compatability.
Modified airflow
characteristics.
Material change for
fuel compatability.
Plastic screen replaced
by metal screen.
Cold start valves pulse
for 8 seconds beyond
start mode/ below zero
degrees centigrade.
-------
1-3
1980 PRODUCTION
METHANOL
Fuel System (Continued)
o Fuel Injection Wiring
o Air Conditioner
Idle Load Compensation
- Ignition distributor
vacuum advance controlled.
o Idle Setting
PCV
IGNITION
o Distributor
o Spark Plugs
OIL COOLING
PCV Valve with calibrated
plunger and calibrated
orifice.
Transistor high energy
with hall effect and
digital idle speed control
through spark advance.
Bosch W175T30
None
Calibration changed for
Methanol.
Material changed for
fuel conpatability.
Modified for cold start
pulse function and to
accomodate relays and
thermo switch.
Throttle body idle air
flow bypass system
controlled. (Same as
1982 Production)
Specific to Methanol
calibration (See
Appendix II)
PCV valve with cali-
brated plunger - no
orifice.
Slightly reduced maximum
centrifugal advance and
slightly modified vacuum
advance/retard char-
acteristics. (See
Appendix III)
- Bosch W260T2-Colder
- Heat exchanged from
engine oil to cooling
water for high loads
only (e.g. trailer
hauling) not antici-
pated to be needed in
normal operation.
-------
ITEM
TRANSMISSION
o Torque Converter Ratio
o Stall Speed
o Gear Ratios
1
2
3
Axle
FUEL TANK
o Material
o Coating
o Seams & Fittings
o Cap
FUEL
1-4
1980 PRODUCTION
- Automatic 3-Speed
- 2.44
- 1900-2200 RPM
- 2.55
- 1.45
- 1.00
- 3.76
- Steel
- Terneplate
- Soldered
- Non-Locking
- Unleaded gasoline
MEIHANOL VEHICLE
Automatic 3-Speed (1981
Production Transmission)
2.44
2000-2200 RPM
- 2.55
- 1.45
- 1.00
- 3.57
- (European)
- Steel
- Phosphated steel,
exterior painted
- Brazed
- European neck and
locking cap
- Methanol with 5.5%
Isopentane
-------
APPENDIX 2
Formaldehyde Measurement
-------
2-1
PCFMAITEHYTE KEASUFEKENT IN VEHICLE EXHAUST
AT MVEL
Robert K. Gilkey
Measurement of exhaust formaldehyde at MVEL is performed using a TKPH (Dinitrophenyl-
hydrazine) technique adapted from that of L.A. Hull1. Exhaust cartonyls (including
formaldehyde) are reacted with CNPH solution forming hydrazcne derivatives. The deriva-
tives are separated directly from the CKPH solution using a liquid chromatograph (LC).
Quantization is accomplished with a spectrophometer in the LC effluent stream driving an
integrator unit which determines peak height and/or area.
SAMPLING SYSTEM
Figure ti gives an overall view of the formal-
dehyde sampling system. Exhaust from the
vehicle is ducted to the constant volume
sampling (CVS) unit where it is quantitatively
diluted with room air. The formaldehyde system
draws off a small portion of the diluted exhaust
through a probe within the CVS unit. The
collection portion is attached directly to the
CVS unit to keep the plumbing as short as
possible. A flew measurement and control unit
is mounted to the wall at the left. The sample
pump is mounted to the floor under the flew unit
and is not visable.
Figure 12 is a schematic of the sampling
system. All of the solenoid valves are electri-
cally connected to the CVS bag sampling
switches. Activation of any one of these three
switches automatically selects a unique set of
inpingers (bubblers) and isolates and vents the
other two sets. Isolation and venting are
required to prevent contamination of the CVS
unit or the satrple lines.
FIQ 1
NCVS
WET T68T METERS
FIO 1
SV-SOLENOIO VALVE
IMP-IMPINOER
The sample system is constructed of stain-
less steel, teflon, and glass upstream of
the iirpingers. This part of the system is
also maintained at 100°C. These precautions
help prevent Joss of formaldehyde within the
system. Downstream of the iirpingers,
construction iraterisls and high temperature
are not critical.
Two ijrpingers are used in each set. Each is
filled with five rcilliliters (ml) of CNPH
solution and imrersed in an ice bath during
test. Two concentrations of this solution
are used depending on the expected exhaust
formaldehyde concentration. 0.25 g/1 DKPH
is used for n;ost catalyst tests while 0.50
g/1 DKPH is used for rcn catalyst tests.
The CKPH is dissolved is slightly acidic
acetonitrile (ACN).
1 L.A. Kull, "Procedures for 2, 4 - Dinitrophenylhydrazone Aldehyde-Keytor.e Air
Analysis". Internal EPA, FTP memo, 1981.
-------
2-2
Tests have shewn that the efficiency of the first impinger is approximately 90% with two
liters per minute sample rate.
ANALYSIS PEOOEUFE
Upon completion of vehicle testing, the impingers are removed from the sampling system and
refilled to 5 ml with ACN. Each iitpinger is permanently marked at 5 irl to facilitate this
operation which restores evaporation loss. The solution is then transferee1 directly to a
glass vial with a teflon lined septum which is compatible with the LC autosampler.
Separation of the cartonyl derivatives is cone using a Waters Associates M-6000A chroma-
tography puirp with a Varian Kicro pak MCE-10 reversed phase 30 on x 4 mm column. A
mixture of 65% ACN / 35% water is used as the carrier at a flow rate of 2 ml/minute. The
column feeds directly' into the primary acsorbance cell of a Varian 635 UV-visitle
spectrophotometer set to 360 nm wavelength. Sample injection is made through a 10 ul loop.
An overall view of the analysis system is shown in figure »3. Ttie system is
semi-automatic. (Baseline drift trust be monitored and corrected during long runs to keep
the integrator from being driven out of its range.)
Quantification is done using peak-height
rather than area. Experiments indicate better
repeatability and more consistant results
with this method. The Hewlett Packard 3390A
integrator permits reports in either
peak-height or area or both.
Standards are run prior to each group of test
vials to be analyzed. At least three are used
to bracket the expected concentrations and a
calibration curve is drawn. Generally this
curve is linear, though corrections are made
if it is not. (Non-linearity occurs when
vehicle test conditions produce concentration
differences greater than two orders of
magnitude.)
Analysis system sensitivity is noise limited
between ± 0.2 and +0.8 ug/ml of formaldehyde
derivative. This translates roughly to 0.2 to
0.8 mg/mi for the FTP test and 0.05 to 0.25
irg/mi for the HWFE test. Repeatability is
approximately i 5% or better.
F1Q 3
Curing test sample analysis, the Cupont 834 Automatic Sampler sequences a flush vial and a
sample vial pair to the injection station. Every sample vial is injected twice. Each
sample is allowed to elute for four minutes before the next injection or pair is intro-
duced. The sampler will hold up to 47 pairs.
-------
2-3
The Hewlett Packard 3390A Integrator is started upon injection of the first sample vial
and allowed to run continuously until the last vial is finished. Ibis unit generates a
continuous trace of the spactrophotoneter output anotated with the apparent retention time
of each peak distinguished. A report is generated at the end of each run. This report
gives peak information keyed to the retention tine. The "formaldehyde" peaks are easily
separated from the others by their relation to the CWH peak. The integrator will hold
information on over 1000 peaks which is adequate for very long runs. A typical vehicle
vial analysis report is shown in Figure 14. Two injections were made of the sane vial.
The peaks at 2.38 and 6.46 minutes are fontaldenyde/CKPH derivative. Onreacted DM>H peaks
are at 1.91 and 6.00 minutes. (All three peaks preceding DNPH are tentively identified as
species of NQc.) (In this case the vehicle was methanol fueled and equipped with a
catalyst.) The total formaldehyde derivative concentration from the exhaust for this test
was calculated as 3.1 ug/nl.
STWJEAPCI2ATIQJ
Standards are made by quantitative dilution
from crystaline formaldehyde/CNPH derivative.
This derivative (Formaldehyde 2, 4-Dini-
trophenylhydrazone) is produced ty reacting
40% aqueous formaldehyde solution with a hot
saturated solution of 2, 4-DWH in methanol.
A drop of HC1 is added and the derivative is
precipitated with water. The crystals are
filtered and recrystalized from a mixture of 3
parts methanol to 1 part water.
Primary liquid standards are made at 500 ug/ml
and 200 ug/nl by dissolving the dried deriv-
ative in HPIC grade ACS. A micro balance is
used for this operation. Successive dilution
of the primary standards is used to give at
least 10 concentrations down to 0.5 ug/ml.
Cnce in'solution, the standards are monitored
for stability.
CALCULATIONS
Data are reported in terms of total formalde-
hyde per test phase and total formaldehyde per
mile driven during the test phase. The
primary equation is:
mgF/rai = (.004046 * CCNC * Vjgp * VKIX).
(VS * C)
HUN * 13
SEP/28/82 05:00:34
HtlCHrt
HT
0.96
i.10
L.64
l.*l
2.38
j.29
4.03
4.44
4.69
5.96
5.19
5.73
6.0U
6.46
6.76
rfelGHT
1S1463
210276
860928
6132900
223822
48386
36025
24962
20429
151201
24649
876831
8201920
232878
2U702
•npi:
PV
L) W
SP8
SP6
dP
W
VP
W
W
W
0 W
aP2
3i
Ibb
0 UP
rtJ
-------
2-4
-------
2-5
"WIX"
"VS"
"W,"
is determined from the formaldehyde peak height courts for each sairple vial. The
"best" peak is chosen from the two for each vial. If both are good, the last is
chosen. The calibration curve for the run is then used to cttain the concen-
tration from the height counts. "Best" is determined from integrator peak
information and visual inspection.
"CCNC"
is teld constant at 5 irl of CNPH sailing solution in each impinger. Evaporation
of the ACN solvent during test is a problem despite the ice bath in which the
impingers are placed. The loss is always made up before the solution is trars-
fered to the sample vials. Transfer of CNPH solution between or out of the
iirpingers cue to pressure imbalances is prevented by the isolating and venting
solenoids.
is obtained directly for each test from the CVS control unit. The value
represents the total volume of dilute exhaust produced by the vehicle during a
test. VKIX is presented at standard conditions of 760 inn Hg and 68.0"F.
is treasured by Precision Scientific 63111 or 63115 wet test meters. The meters
are calibrated at nominal KVEL pressure and temperature conditions cf 736 irm Hg
and 73 "F to correct readings to the above conditions. Corrections to actual test
conditions are minimal and are neglected.
is obtained as roll revolutions from the dynamometer control unit. A calibration
factor is used to convert this reading to miles. This calibration rarely changes.
(Molecular Weight) for both formaldehyde and its DNPH derivative were calculated
from their irolecular formulas and generally available atomic weights. The
formulas are:
2, 4-Cinitrophenylhydrazine (CNPH) ........ H2 NNHCgH3 (N02'2
Formaldehyde .............................. OCH2
Formaldehyde 2, 4-Dinitrophenylhydazone... CH2 NMKgH3(hJC2>2
Cne mole of formaldehyde reacts with one mole of CNPH to give one irole of
derivative plus one mole of water.
A standard work sheet is used to collect data and report results. The results may be
calculated from the equations and conversions given on the sheet. A "BASIC" program for
the apple Computer has oeen developed to complement tne work sheet. This program generates
a calibration equation of the form: Cone » A3* (Counts) 2 •»• A2* (Counts) •»• 0. The curve is
forced tnrougn zero, zero. The coefficients are then used in the reduction program pre-
sented in Figure 8.
-------
- (.004046 * Cone *
VDUB * vmx>/
FORMALDEHYDE ANALYSIS WORKSHEET
TEST t
UAiX
DMPH Vol . '
Snmp. Vo 1 . >
4
VM1X ,
i
Distance t
(Cal.) •
Distance >o
lU'fl. ,i
Range • >
Haw Ct>nc. '•
Hag Cone. .»
Hag Cone. ,,
Tot . CH2O „
jo
CIUO Emlss ,,
7T
Wt . FTP .,
.-
>s
'•
>•
„
10
iCOMVERT
* 28.J16
/(RR/ml)
Dist
* Mt
lot. CH20
* Wt
t UNITS .
ml
ft3
1
ft3
Roll Rev
ml
ueo/ul
ppmF
mgr/l
n.gF
mgp/nii
ml
Wt ml
D,g.
Wt Tot
iWt- Tot
1
VliUB
VS
WIX
Dlst
Cone
CII20 E.
• i>e i
0.5
0.43
< B|> 2
1.0
1 .00
• Bg 3
.
0.5
0.57
» FTP Tot
t
'
. IIUFE
sr
oil l
2 3. tQ
4-ilF"
J?S4J
X33I-S7
10-tlf
Ji3*t*9V
*»«• O.f
3.13
11.041
/./
. iuu:.
..20 cnph
>.V> Bpll
i/iO uph
FIG e
11
10
I
-------
2-7
]RUN FMALD.EPA
FORMALDEHYDE DATA REDUCTION
CAL DATA
A<1 ) = 0
A<2) = 9.55983598E-06
A<3) = 1 .59070037E-12
ARE THESE THE RIGHT CQEFF'S ? (Y/N) Y
TEST DATA
USE 'Q' TO QUIT 'R' TO REDO
DNPH VOLUME (ML) ? 5
VB • 5 ML
SAMPLE VOL
-------
2-8
3LOAD FMALDPRKO
JUST
20 HE* * "FORMALDEHYDE DATA REDUC
TION"
30 REM : PR*4
40 HTAB 20 - < LEN / 2*> : PRINT
HE*: PRINT : PRINT
80 INVERSE : PRINT "CAL DATA": NORMAL
: PRINT
100 NS = 3
102 D* = CHR* >:•»>: REM CONTROL
104
106
108
110
112
114
1 16
113
120
140
160
180
200
220
240
260
262
264
266
268
280
PRINT 0»!"OPEN COEFF. L45"
PRINT D*;"CLOSE COEFF"
PRINT D*s"OPEN COEFF, L45"
FOR II = 0 TO NS - 1
PRINT D*!"READ COEFF, RO , B"
;I1 » 15
INPUT ASdl * 1) : NEXT II
PRINT D»:uCLOSE COEFF"
'GOTO 200
INPUT " A<1) « ";AS<1)
INPUT " A<2) =» " ;AS<2)
INPUT " AO> = " :ASO>
PRINT
INVERSE
NORMAL
PRINT "CAL
PRINT
";AS<1>
" ;AS(2)
";AS<3>: PRINT
HOME
DATA"
PRINT " A<1)
PRINT " A(2)
PRINT " A<3)
: PRINT
INPUT "ARE THESE THE RIGHT C
OEFF'S ? (Y/N) ";IN*
IF IN* » "N" GOTO 120
IF IN* < > "Y" GOTO 262
PRINT : PRINT
HOME : INVERSE : PRINT "TEST
DATA": NORMAL
PRINT : PRINT
290 HTAB 10: PRINT "USE 'Q' TO Q
UIT 'R' TO REDO"
291 PRINT : PRINT
300 INPUT " DNPH VOLUME 'JML.' "> "
320
330
335
340
360
365
370
380
390
400 ','
IF VB* = "" THEN U8* = "5'
IF MB* •• "Q" THEN END
IF >,'B» = "R" THEN PRINT "*•
": GOTO 280
IF VB» = "5" THEN GOTO 400
INPUT " VALUE IS NORMALLY 5
- IS YOUR VALUE GOOD ? (Y/N)
" : I N*
PRINT "CHR* <7>: PRINT CHR*
<7> REM SELL
IF IN* = "5" THEN IN* = "5":
GOTO 400
IF IN* = "N" THEN GOTO 300
IF IN* <: > "Y" GOTO 300
8 = 'JAL : PRINT " VB =
B:" ML": PRINT
Fig. 8
-------
2-9
420 INPUT " SAMPLE VOL vCU FT OR
L) ? ":VS»
430 IF VS* = "Q" OR VS» - "R" THEN
PRINT "»*": GOTO 280
433 IF VAL (VS*> - 0 THEN PRINT
"ILLEGAL VALUE-PLEASE REENTE
R": GOTO 420
440 CK*(1) - -FT3"
440 CK»<2> * "FT"
480 CK*<3> = "F"
500 IF RIGHT* (VS»,1> « "L" THEN
VS - VAL (VS»>: GOTO 660
520 :
540 FOR I » 1 TO 3
560 IF RIGHT* (VS*. LEN (CK»(I)
)) = CK*(I> THEN VS * VAL <
VS*> » 28.316: GOTO 640
580 NEXT I
600 IF VAL (VS*> > = 8 THEN US
= VAL (VS*>: GOTO 660
620 VS » VAL (VS«) » 28.316
640 PRINT " VS » " ! UAL (VS*):"
CU FT"
460 PRINT • US =• "sySs" LITERS":
PRINT
680 INPUT " VMIX
690 IF yM« - "Q" OR lvW* - "R" THEN
PRINT "»»": GOTO 280
700 PRINT " yMIX = ":i,!M;" CU FT"
: PRINT
720 INPUT • ROLL REVS ? ":RR*
723 IF RR* » "Q" OR RR* » "R" THEN
PRINT "»»": GOTO 280
730 IF VAL (RR*) = 1 OR VAL
-------
PREPARATION
AND SAMPLING
ANALYSIS OF
SAMPLES
STANDARDS
DATA REDUCTION
Mix DNPU Solution
.25 i;/l or
.50 g/1 DNl'll
in ACJ
Fill 2 Imp infers
per Vehicle test
wila 5 ml solution.
Connect 2 impingers
In series per set.
I'lace sets in ice.
Connect sets to
sample system.
Zero wet test meters.
Turn on system.
Sample Vehicle exhaust.
Sets selected with
"dag Switches"
T
lie cord
V
imp
VS
VMIX
Hull Uevs
Test 'Type & lumber
O.ite
lU'store 5 ml is
impingers with ACM
Fill and mark vials.
(one vial per irapinger.)
I ill flush vials with ACM
Load autosarapler
Standards in decreasing
concentration. (>•» 3)
Sample vials in test
sequence
All samples separated by
flush vials.
I I'nin on and set equipment. |
Uun Standards - Manual Mode
(Single injection)
Kun Samples - Automatic Mode
(2 injections)
Kocord
Order of vials.
1'eak Height Counts for
each vial and injection.
Comments
Prepare crystaline
FormaIdehyde/DHPH
derivative.
Prepare
standaril:> by
quantitat ive
dilation with
ACN.
Record
Hxact concentration.
Date prepared.
Date of crystals used.
i* ('.il (inrv
:li run.
uci'iii i iii ion lor
each sample and
inject ion.
SeJ.-ct "host".
Ueduce concent rat in
values tn test
values.
(mg formaldehyde
per test, or
mg/mi.)
I
t->
o
lltcport Ue:iuli::;l
-------
2-11
Procedures for 2,4-Dinitrophenylhydrazone Aldehyde-Ketone Air Analysis
L,A« Hull, Dept. of Chemistry, Union College, Schenectady, New York,
on leave at U.S. EPA, in Gas Kinetics and Photochemistry Branch
Mail Drop 84, RTF, N'C 27711
I. Raagents;
A. 2,4-Dinitrophenylhydrazine (DNPE) - Ccomercially available DKPB is
reerystallizad 2-3 times from HPLC grade acetonitrile (ACN)(Burdick and
Jackson). To 50 ml of the ACN is added 3 gms of the DNPH. The solution
is brought to a boil and decanted from any solid residue, allowed co
cool co room temperature and then placed in an ice bath. The crystals
are isolated by suction filtration with a mi^nim of atmospheric exposure
to prevent the introduction of contaminants.
B. Sampling Solutions;
1. Ambient sampling (lov ppb levels): In a 1.0 1 volumetric flask
0.25 g of purified DNPH is dissolved in 1.0 1 of HPLC grade ACN.
To the resulting solution is added 0.2 ml of concentrated H.SO,.
2. Laboratory sampling (ppm levels):
doubled.
The above concentrations are
II. Sampling Procedures;
A. Apparatus; A schematic of the apparatus is shown in Figure 1. The
pump, flow controller, and flow meter all come after the impinger. The
impinger is a non-frit type with the bubble tip within 3.0 mm of the
bottom. The impinger should be calibrated for 2.0 and 4.0 ml of solution.
B. Ambient Samples; Without the bubbler the flow rate is adjusted for
about 0.5 1/min with the needle valve. To the impinger is added 4.0 ml
of the "ambient" sampling solution. The iopinger is connected to che
pump and the inlet lines and placed in an ice bath up to the level of
the DNPH solution. The pump is Chen turned on and che flow readjusted
to 0.5 1/min. The sampling continues for 60 minutes (30 liters). After
Figure 1. Schematic of DNPH sampling apparatus
-------
2-12
sampling is complect th« impinger is disconnected from the pump and
inlet lines, caped and the solution waned to room temperature. With
the caps off the impinger the solution is made up to the 2.0 ml
nark on the impinger by the addition of ACM through the inlet portion
of the lipinner.' This serves to fix the final volume for concentration
calculations latter and wash any material that collects before the
sampling s.olution into the solution. The solution is then transferred .
to a cation caped vial.
C. Laboratory sampling; The apparatus is the same except no ice bath
is needed. Only 2.0 ml of DNPH .laboratory sampling solution is required
in the impinger and the sampling rates are from 0.1-0.5 I/minute with
the total volumes from 0.25-2.0 1 depending on how high the concentrations
are. With the solution as constituted it would be best to keep the product
of the carbonyl concentrations times the volume sampled less than 10 ppm-
liters (10,000 ppb-liters) and the optimal product is 0.50 ppm-liter. For
example if the carbonyl compound is at 0.5 ppm then a good sample size
would be 1.0 1 with the maximum being 20. liters. Another limitation
arises if an accurate analysis of ketones is desired. In that case the
amount of moisture introduced must be kept less than 50 microliters in
the 2.0 ml of solution. The sampling volume may then be determined by
taking into account the humidity of the air. After sampling the solution
is made up to 2.0 ml with ACM addition (as described befdte) and then
transferred to a teflon caped vial.
III. Analysis;
A. Standardization; Standards can be prepared in two ways.
1. Solid 2,4-Dinitrophenylhydrazones: Using standard methods (N.D.
Cheronis, J.B. Entrikin, and E.M. Hodnett, Semimicro Qualitative
Organic Analysis, 3rd Ed. Interscience Publishers, New York, 1965,
pg. 499-501) the crystalline 2,4-dinitrophenylhydrazones of a
number of the ketones and aldehydes were prepared. Weighed samples
were then made up to known concentrations in ACN solution (approximately
2. X 10 M) and the solutions used as standards.
2. Direct addition cif_ the carbonyl compound jrp_ the reagent solution;
A measured volume of a liquid carbonyl compound (usually 1.0 micro-
liter) 'is added to ACN (2.0 ml). An aliquot (usually 4.0 microliters)
of that solution is then added to 2.0 ml of the laboratory sampling
solution. Using the density of the carbonyl compound the concentration
of the carbonyl compound (actually the 2,4-dinitrophenylhydrazone
derivative) in the sampling solution can be calculated and the resulting
solution used as a standard.
B. Analytical conditions; A Varian 5000 EPIC liquid chromatograph
equipped with a built-in 254 am ultraviolet absorbance detector connected
to a Hewlett-Packard 7132A recorder, and a Variable Wavelength Spectra Physics
SF 770 UV detector (set for 360 nm) connected to a. Hewlett-Packard 3380S
integrator were used. The analytical column was a Varian Micropak MCH-10 re-
versed phase 30 cm x 4 mm column. The analytical conditions are similar to
those already described (K. Kuwata, M. Uebori and Y. Yamasaki, J. Chrom. Sci.,
17., 264 (1979)). The HPLC conditions were 65Z acetonitrile/35Z water
-------
2-13
(currently the analysis is done with 641 acetonitrile/362 wacar to
compensate for soma column dagration) with a flow rata of 1.5 al/min.
In Table. 1 are list ad tha retention times and calibration factors for
those common compounds for which standards have been run. The
standardization factors are based on a 30 1 air sample having deposited
ics aldehydes/kecones in 2.0 mi of che ONPR reagent solution. For
smaller air samples or larger volumes of collecting solution proportional
factors can be used with the standardisation figures in Table 1. In
Table 2 are listed the retention times and standardization factors for
soma terpene carbonyl compounds run with solvent programming as
follows: flow 1.5 ml/min, 65Z ACS/H.0-5 minutes, 65 to 75Z ACS over
the next 10 minutes.
C. Analytical Procedures ; The sample solutions are transferred to a
heavy-vailed 2.0 ml reaction vessel fitted with a teflon cap (Supelco,
Inc., Belief onte, PA) and heated 15 mins in a water bath at about 70-
80 C. The solution is then injected into the HPLC via a 10 microliter
sampling loop. The solution is heated for another 15 minutes and
the analysis repeated until successive injections agree to within
10Z. For aldehydes the development is usually complete in 10-15 minutes.
For simple ketones 30 minutes usually suffices, while the dicarbonyl
compounds require as much as 3 hours heating.
Using the standardization factors and retentions times the peaks can
be assigned and quantified. Because the formaldehyde peak overlaps the
tail of the unreacted DNPH reagent the integration obtained is often
distorted by baseline triggering problems. For a reliable formaldehyde
concentration it is best to draw a baseline and use the absorbance
measurement to determine the concentration.
1. Ambient samples ; Because all the ambient samples are likely
to contain significant quantities of water (greater than 0.2 ml)
the ketone responses are virtually completely suppressed by the
equilibrium shown below while the
xc - o * HZN-NHDNP » c - NNBDK? + H2o
aldehyde responses are approximately 90Z of their true, ambient
values. This result was obtained from experiments in which
water was deliberately added, as well as sampling from moist
bag samples. The data on ambient samples can Chen be handled
as all aldehyde analyses and the values obtained as being approx-
imately 90* of the true ambient values.
For high boiling (greater than 150-200°C) ketones (in particular
the terpene carbonyl compounds) it is possible to evaporate off
all the solvent (ACJI and water) from the sample solution by
gently heating the solution in a 10 ml beaker on a hot plate (remove
the solution before the last of the solvent evaporates and let it
do so without further heating). Redissolving the residue in 2.0
ml (or less, if enhanced sensitivity is desired) pure ACN removes
the water interference problem.
-------
2-14
2. Laboratory samples; If the quantity of water in the sample
(as determined by the humidity of the sampled air and the volume
sampled) is less than about 50 microliters/2.0 ml of sampling
solution there is little if any interference in the analysis of
any" aldiihyd'e or ketone so far sampled. Using 2 bubblers, bag
.sampling, and FT-IR. cross checking of concentrations indicates
collection efficiences are 100% as far as it can be determined for
ail che varieties of caapounds Listed in Tables 1 and 2 from Che
Lou ppb range up co several ppm.
3. Interferences; Besides the vater interference in ketone analyses,
as mentioned above, there is also a potential interference of simple
aromatic compounds with the HPLC analysis at 254 nm. Because the 254
UV absorbance detection is Sensitive to the. presence of aromaticity,
any species that collects in the ACS solutions and possesses an
aromatic ring can potentially interfere with the 254 nm analysis.
As a practical matter only benzene, toluene, (RT 3.74 min) and the
xylenes (RT 4.5 min) are likely interferences. The 254 detector is
1/25 as sensitive to the above compounds as to the DNPH derivatives
so only high concentrations would interfere with the analysis of
particular carbonyl compounds. The use of 360 nm detector eliminates
any such potential interference.
In experiments to date no interferences of 0. (less than 0.5 ppm),
NO (less than 5 ppm), NO, (less than 5 ppm), and BONO (less than
5 ppm) have been observed in the 1-2 liter laboratory sampling
and none have been observed with ambient sampling.
IV. General Comm-:--!ts; The above described method for ambient aldehyde and
laboratory aldehyda/ketone analyses is simpler than the aqueous impinger method
described in the literature (see above, K. Kuwata reference) since it involves
no extractions (which introduce solvent contamination problems and small
volume handling problems) and in addition is efficient at collecting and
quantifying carbonyl compounds of six or more carbons. In tests of the
aqueous impinger method it was found to give, in our bands, less than 10Z
of che known gas phase concentration of benzaldehyde. Also even for high
concentration ("laboratory") runs on ketones, because of the presence of water
(as solvent) che aqueous impinger method was not useful for ketone determinations.
While che above described method has drawbacks ic is a useful tool for ambient
aldehyde measurements and quite useful for aldehyde/kecone measurements in
experiments where the water concentrations relative co che aldehyde/ketone
concentrations are in che appropriate range.
The use of 360 nm detection (instead of 254 nm) also improves che sensitivity
of che analysis. The increased sensitivity could allow L5 L ambient samples or
30 min sampling time and ic eliminates any potential interferences from simple
aromatic compounds. For laboratory analyses chis will increase the sensitivity
for which there is no water interference.
For routine analyses of high concentration samples (auto exhaust for
example) where carbonyl compounds may be 1-10 ppm range it should be possible
-------
2-15
to use 10-20 ml of the DNPH/ACN sampling solution ("laboratory") and collect
1-2 liters of txhaust ovtr soaa convenient time (30 minutes). The resultant
DHPH derivative„concentrations should be ample and the vater interference
.g-injmqT (assuaing'the water is less than about 250 torr).
Care oust be taken in the sampling co not unduly obstruct the flow of
air into the sampling solution. Ic has been observed that significant
decreases in the aldehyda/keroae concentrations (when in che ppb range)
are observed if the gas sample passes through a simple 1 micro teflon
filter.
-------
2-16
Table 1* Retention Times and Calibration Factors for Simple
Aldehyde/Ketone 2,4-Dinitrophenylhydrazones
Compound ~ *
(DNPH derivative)
2,4-ONPH
Formaldehyde
Acetaldehyde
Pr op ionaldehyde
Acetone
i-butyraldehyde
methyl vinyl ketone
crotonaldehyde
methacrolein
methyl ethyl ketone
cyclopentanone
glyoxal
benzaldehyde
cyclohexanone
o-colualdehyde
methylglyoxal
hexanal
biacetyl
Retention
Time (Mins)
254 nm
2.47
3.22
3.77
4.51
4.46
5.40
5.15
5.20
5.29
5.70
5.75
5.98
6.45
6.88
7.51
8.25
8.72
11.75
Absorption Cal. ,
(ppb/Abs. unit, x 10 " )
254 run
—
2.92
3.60
4.91
4.54
4.84
4.74
4.00
4.17
5.50
6.3
4.40
5.94
6.20
7.76
5.50
9.47
9.00
Integration
(counts/ppb)
254 am
—
1358
1313
1128
1224
—
1540
1819
1651
1248
1287
2066*
1433
1426
1417
2066*
1228
2066
Integration*4
(counts/ppb)
360 nm
—
5437
5396
4726
5033
6327
—
5958
6393
5138
—
3502*
4929
—
4331
3502*
5357
3502
**
Biacetyl was used as a reference to standardize these compounds which come
as aqueous solutions.
The retention times on the 360 nm detector are 0.1-0.3 minutes longer than the
254 detector since the 360 detector is "downstream" from the 254 detector.
-------
2-17
Table 2. Retention Times and Calibration Faccors for
Terpene Carbonyl Compound with Solvent Programming
Compound
(D*r?H derivative)
c-pinonic acid
c-p inon«ld«hyd«
(mono ONFB)
nopiaone
c-p inonaldehyde
Retention
Tia« (ains)
25* na
4.02
5.5A
10.0
13.60
Absorbance Cal.
(ppb/Abs, X 10" )
25- na
4.18
—
9.83
5.42
Integration
(councs/ppb)
254 na
1478
—
1012
1717
Integration
(sounts/ppb)
260 na
5114
—
3766
8629
-------
APPENDIX 3
Fuel Analysis
-------
suuihLWhbi KhbE ARCH INSTITUTE
»O»TOMICI OAAWfft 2M10 • «220CUt.«S*A AOAO • SAN ANTONIO. TIXA3. USA 7t2»4 . iSI2I 444.4111 .riLIX 78-73S7
May 6, 1983
Mr. Carl Scarbro
EPA
2625 Plymouth 3d.
Ann Arbor, MI 43105
Dear Mr. Scarbro:
V« have conplaced che :ascs you requesced on vour 3acch 100
aechanol samnle. The resales were:
Tes- Results
Heac of Coabuscion (ASTM D-24Q)
Gross 10,292 3cu/lb
Nee 9,143 3cu/lb
Wacer Concenc by Sari Fischer Ti:racion 0.0553
(ASTM D-174A) we. S
API Gravi;-/ (ASTM D-237) ' 46.9° 3 60°T
Densir/ (ASTM D-2S7) 0'. 7923 .? 15°C
Flash Point (ASTM D-93) 71.9°7
Acid. Mumber (ASTM D-66u) aquiv. ag KCK/g sanspia 0.00
lead by A.A: (ASTM 2-3227) 3 ppm
Sulfur by Dohraann ^'lisrc
Phosphorous by A.A.
Signer Alcohols by G.C. :,M. ;<0.1," aa.)
N.O.: Mone cecactad
ANTONIO. T;XAS
a t > < e t t ' * » a u « r 3 «. rii*j. » • o «»«»i»aro» 3 :
-------
Jlr. Carl Scarbro
Page 2
May 6, 1983
All the above cases vera performed in cuplicaca and :ha averases
reporcad. The prices billed far :hese tascs reflect an across-che-
board price increase for our Division vhich becaae effective on
October 1, 1982. As I aencicned in our calaphone conversation, ve
performed ihese analyses las- Novesber (1982), buc have held the
rasul'S pending approval of paymenc-ir.-full for a previous purchase
order (No. A-0579-MNSX) performed for Mr. 3ill Clanaens, also cacir.g
from lasc Movessber.
Iz you have any further questions, you ^ay call r.e ac (512)
' '
Sincerely,
Joseph Brock "ischer
Research Sciencisc
ingines , Fuels i L-bricancs
Depc. of ?ecrola-ja Research
-------
APPENDIX 4
Individual Test Data
-------
NIIMUEK (12 CAI/K
DAI t
DOOM I PRO
ALOY
MI'G
IIC
CO
CO2
NOX IIC-NM ME I HANOI
SIOCK CAIAlYS
BI-I2IO 9 SIOCK
S 1-12 1 1 9 SIOCK
B 1-12 12 9 SIOCK
814597 9 SIOCK
8 14678 9 S IOCK
SIOCK CAIAI.YSI
BI5I25 3 SIOCK
SIOCK CA 1 Al YS 1
815163* O SIOCK
8 I52O6 O SIOCK
NO CAT Al YSI
8 15236» O NONE
8 15238 O NONE
8 I524O O NONE
NO C A F A 1 Y S I
8 152-18 3 NONE
8 I525O 3 NONE
8 15254 3 NONE
NO CAI Al YSI
8I526O 5 NONE
8 15262 5 NONE
815264 5 NONE
4X6 12 : l(# 1 I
8 15272 O (» 1 (
8I599O O <»l)
8 15992 O (H»
4X6 12 : 1 ( H }
815995 3 (M\
8 15997 3 ( * 1
815999 3 (H\
4X6- 12 : l( * )
BIGO03 5 <»l
8I6OO6 5 (#1
8 I6OI 1 5 ( # 1
8 I6OI4 5 ( * 1
Nil C A 1 A 1 Y S 1
u luoi'o o tint it
H I6O22 (J NOHt
C, 23
G 24
b 29
7 08
7 O9
3%
/ 30
()'/,
a 03
8 O4
oz
8 IO
a 1 1
a 12
3%
a ta
a 20
a 24
5%
a 2/
9 oa
9 O9
()"/.
U 15
917
it 2 1
3%
9 24
9 28
9 29
5'X.
u :)o
IO 05
IO OG
H) O7
o-X.
10 1:1
10 14
a2
62
82
82
82
O2
82
O2
82
82
O2
82
82
82
O2
82
82
82
O2
82
82
82
O2
82
82
82
U2
82
82
82
O2
82
82
82
82
(12
U2
82
26O5
2624
2652
2908
291 1
2987
??
30O6
3OI8
3056
3 IO5
3 144
3257
3286
3356
3453
3492
354 1
3682
3768
:iao7
386 1
39OI
394O
4O03
4 1O5
4 124
4 183
428O
43 19
O
O
4
0
O
O
O
O
0
O
4
O
0
7
7
0
7
1
1
0
9
5
O
5
0
O
4
O
O
F IP
f IP
F IP
F IP
F IP
F IP
FIP
F1P
FIP
FIP
FIP
FIP
F rp
FIP
FFP
F IP
FIP
F IP
F IP
F IP
FTP
FIP
F IP
F IP
F IP
F IP
F IP
1 IP
F IP
20 2
17 4
172
N/A
N/A
15 4
27 1
26 3
353 5
322 9
313 B
259 1
281 3
252 6
185 0
189 1
197 8
a 5
13 2
13 2
17.5
12 9
16 4
18 9
20.9
22. 1
22 O
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•1X6- 1OO|J()( //
817-495 5 (44)
817199 5 (//I)
8 179 19 5 (//-I)
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NUMUEK O2 CAI*
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MPG
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CO
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B 142 16 9 SIOCK
814219 9 SIOCK
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NO CAIALYSI
815237 0 NONE
8 15239 O NONE
8 1524 1 O NONE
NO CAIALYSI
815249 3 NONE
8 1525 1 3 NONE
815255 3 NONE
NO CAI At YSI
B 15261 5 NONE
8 15263 5 NONE
815265 5 NONE
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8 15273 O (/ft)
8 15274 O (* 1 )
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8 I6O2 1 O NONE
8 16023 O NONE
NO CA 1 At YSI
8 1 6O2 V 5 NONE
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0
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tJt
12
12
12
12
12
12
12
1
1
1
1
1
1
1
1
1
oy. 02
Ol 82
-O7 82
O8 82
O% O2
14-82
15 82
3% 02
16 82
17 82
-2 1-82
5% O2
O4 83
O4-83
o% 02
O5-B3
o% 02
O6 83
12 83
3% O2
13 83
14 83
5-y. 02
18 83
19 83
bO27
5137
5188
5319
5338
540O
5448
5499
5598
56O9
5662
5674
5805
5865
5912
5966
6OI7
0
O
O
O
O
0
O
O
6
O
O
O
O
O
O
6
0
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDl E
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
19 96
13 46
12 45
N/A
N/A
N/A
N/A
1O. 38
49.64
56 26
6.98
14 16
< O 45
4 O4
1 1 16
26 82
29. II
137 O
136 O
142 O
134 0
132 O
1 15 O
1 12 O
124 O
1 1 1 O
12 1 O
IO9 O
1 19 O
121 O
123 O
124 O
121 0
1 16 O
0
O
O
O
O
O
O
O
O
0
O
O
O
O
O
0
0
O94 1
1 1 17
O882
O027
OO47
OO58
0715
OI92
O359
.O7O9
. 1591
1371
OO24
OO44
OO8I
OO98
0164
O 5186
O 6316
O 64O7
O OO27
O OOO3
O.OOO1
O 27 12
O O56O
O OO29
O O056
O.83I3
0 4931
O OO29
0 OOOI
O OO3I
O O084
0 0026
28
28
27
3O
31
35
36
33
36
33
36
33
33
33
33
34
35
956 O
825 O
786 O
789 O
289 O
781 O
O91 O
1 16 O
884 O
7 IO O
002 0
535 O
894 O
394 O
179 0
051 0
412 O
0258
O29O
O332
.OO93
OO52
O237
O329
O246
OI4 1
OI88
O456
024O
OO4I
OIO8
OI23
OO82
O224
O
O
O
O
O
O
O
O
0
O
O.
O.
. O937
1 1 13
O87O
N/A
OO4 1
OO51
O7O8
0183
N/A
N/A
N/A
N/A
OO17
OO38
OO66
OO86
O149
O 2956
N/A
N/A
N/A
N/A
N/A
N/A
O O342
N/A
N/A
N/A
1
I-1
O
O 4315
N/A
N/A
N/A
N/A
N/A
4X6 lonl'lH «-l
81792O O «»4)
O'/. O2 AGAIN
I 2b 83 6O66 O IDLE
I I 59 119 O O.OI39 O.OO29 34 632 O.OO84 O O13O
N/A
NO CAIAI.YSI
817923 O NONt
oy. 02
I 27-83 6116 O IDIE
24 12 N/A O 1133 I.O47 N/A OO242 O 1122
N/A
4X6 I'llUMI Vb I
817927" O <*b)
8 I 7 9 3 I i O < // b )
oy. 02
I 2H-B3 6168 O I DIE N/A N/A
2 Ol 83 6222 O IDIE N/A N/A
O O724 O 4728 N/A O O2I I O O716
O IO84 O 5IIO N/A O O259 O.IO73
N/A
N/A
4X(i l'l)ISM(v'o»
II I /'.l.Jft • :» ( '/b (
:r/. 02
2 O-> B3 6277 O IDIE N/A 132 O O O997 O 6692 29 87 1 O O299 O O986
N/A
-------
-IXG
81794 1
fl l/b 15
IXG
8 17949
8 I79b3
4X6
8 18394
8 18398
I'llUMC #5 )
0 (//S)
O ( '/ 5 )
POIJMC #5 1
3 ( // 5 )
3 <
0 I//8)
AG( //a \
3 8)
3 ( //a )
(IX.
2 09
:>. 10
37.
2 1 1
2 IS
57.,
217
2 18
07.
2 24-
2 25
37.
3 Ol-
3 O2
57o
3 O3
3-O4-
07,
3 IO
3 1 1
315
3%
3 16
317
57.
3 18
3 22
3 23
07.
4 O7
4 OS
3%
421
•I 22
02
83
83
O2
83
83
02
83
83
02
83
83
O2
63
83
02
83
83
02
83
83
83
O2
83
83
02
83
83
83
O2
83
83
O2
83
83
6425 O
G-177 0
6533 O
GS87 0
6G85 O
674 1 O
687 1 O
6927 2
6997 O
7047 7
7 IO4 6
7 156 O
7288 7
7345 O
7396 O
7452 O
75O4 O
7561 O
761 1 O
7663 O
797 1 O
8O23 O
8254 O
8326 8
IDLE
IDI £
IDLE
IDLE
IDI E
IDLE
IDI E
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDLE
IDI E
13 24
13 38
- 1 0
1 O
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
- 1 .O
- 1 .O
-1 0
N/A
- 1 O
- 1 O
- 1 O
1 36 O
N/A
N/A
128 .O
1 18 0
123 O
127 O
124 .O
1 18 0
121 O
1120
1 18 O
124 O
IO9 O
127 .O
124 0
126 O
123 O
123 0
1 19 0
132 O
123.0
IO4 .O
122 O
0 O8O5
O O897
O O999
O 1222
O 1337
O 1365
O 1473
O 1436
O 161 1
O I4*OI
O 1566
0. I7O5
O O272
O 0766
O OO15
O O1 16
O O075
O.O233
0 02O7
0 O287
O O663
O O4 15
O 1259
O O538
O 3648
O 4 169
O 4517
O 4O59
O 642O
O 6OO9
0 5354
O 6254
O 59O7
0 8202
O 6746
0 57 1 1
O 2243
O 1233
O O677
0 0023
O OO83
O OO28
OOO55
O OOO1
O 4556
O 4889
O.B4OO
O 7222
29 361
N/A
N/A
31 26 1
33 424
32 OI4
31 234
31 716
33 317
32 273
35 I9O
33 575
32 69O
37 319
32 199
33 168
32 526
33 275
33 326
34 . 482O
3O 292
32 6374
37 .7738
32 4326
O O244
O O2 31
O O244
O O299
0 0456
O O43I
O O329
O 0262
O O264
0 0279
O O3O2
O O296
O OO66
O OI27
O OOO8
0 0155
O O229
O O243
O O235
O O27 1
O OI98
O.OI87
O O24 1
O.OI64
O.O795
O O889
0 0982
O. 1218
O 1318
O. 1353
O 1458
O. 1421
O. I6O4
O. 1391
O 1547
O. 1698
O O26O
O O75O
O OOO5
0 0109
O OO63
O.O2I9
N/A
N/A
0.0655
O O4O2
O. 124 1
O.O523
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
-------
NUMBER O2 CAI*
DA I I
OOOM 1PRO
AlOY
MPG
HC
CO2
NUX HC-NM
•1X6- 12 : \(H \\
8 16032 O ( * 1 )
8 15993 O ( 1 \ )
4X6- 12 : \(H \ )
8I6OOI 3 (//I)
4X6 12 t(# 1 )
8I6OO5 5 (»l)
BI6OO7 5 (#1)
8I6OO9 5 (*l)
4X6- 12 : MH \ )
8I6OI6 3 (»l)
8I6OI8 3 (//I)
NO CAIALVSI
8I6U24 O NONE
6XRIO 12 : M *2 )
8I6O29 O (#2)
8I657O O (#2)
6XRIO- 12 : l<*2 >
816578 5 (ft 2)
8(6582' 5 (#2)
NO CAI At YSI
8 I6t>92 > O NONE
8 16598 O NONE
8 I66O2 O NOME
•1X6 3:2 (*J)
0166 IO O (//3)
816612 O (»3)
4X6 -3:2 ( #3)
816615 3 t*3)
816619 3 (//3)
8I746O 3 •) B3
3747
3818
397 1
4032
4O45
4O78
O SS IO
3 SSIO
8 SSIO
O SSIO
O SSIO
0 SSIO
1 .9
O.2
1 3
1 .8
3.7
5.8
IO O
IO 1
10 1
10 1
96
IO 1
O O28
O 012
O O22
O OI9
O O25
0 O25
00
O.O
0 OI6
O OI6
O.O
O.O
412 O9 1
407 333
407 998
406 680
430 273
406 958
O OIO
O O45
0 284
O 331
O 295
0 302
O.O26
O.OO2
0.009
O.O07
O.O12
O.OI2
(AGAIN)
4228
4233
4351
4444
4623
4765
482O
5027
5137
5 188
5319
5338
54OO
5448
5499
5598
\\\\
3 SSIO
2 SSIO
0 SSIO
0 SSIO
2 SSIO
O SSIO
0 SSIO
O SSIO
O SSIO
O SSIO
O SSIO
0 SSIO
O SSIO
0 SSIO
O SSIO
6 SS IO
\ S5 IO
4 7
117
IO9 2
02
2.O
1 .8
2 7
133 4
IS) .2
129 4
N/A
N/A
N/A
N/A
64 .BO
293 Ob
294 . 49
IO.3
tO 4
IO 2
10 5
IO 2
IO.O
95
9 6
99
IO O
10 2
98
9.7
9.6
9 8
98
-in
O O38
O O24
O 427
0 O20
O 021
O O23
O O27
O 4 12
O 396
O 433
O O22
O.O4O
O.O25
O 090
O 038
O IO2
-in
0 O34
O 033
11 387
O 0
O O
O OI8
0 020
8 879
9 7O6
to 4oa
O 235
O 154
0 001
0 222
O O
O (X)l
- i n
382 462
394 687
382 462
39 t 84O
4O2 966
4 I3.O33
433 838
4 15. 744
397 574
394 668
4O4 822
4 18 2O7
424 8 16
429 683
42 1 .589
421 831
- 1 O
O 301
O 285
0.261
O 196
O 267
O 3O4
0.290
O 331
O 33O
O 335
0 045
0 041
O 279
O 339
O. 3O8
O 258
i n
O.O25
O.OI3
O 4 15
O OIO
O.OI 1
O OI4
O 014
O 4OI
O 387
O 4 19
N/A
0.03O
0 013
O.O75
0 O23
N/A
•• i n
MEIHANOL
O O6O
o.ooa
O.OO7
O.OO7
O.OI3
N/A
O.OO6
O.O09
O46
O 161
N/A
O O22
O Oil
I 174
N/A
N/A
N/A
N/A
N/A
N/A
O O36
N/A
Ml) (, A I AI Y 'j
-------
817-172 O NUNt
I 05-B3 5662 O SS IO 106 85 99 O 528 IO 429 396 796 0 365 N/A
N/A
4X6-
U 17 4 / 4 9 ( /' 4 >
8 17482 O (*4 )
1X6 IOOf'01 * I )
817486 3 ( /X4 >
BI749O 3 (//-))
•1X6- IOOITH »4 )
817-193 5 1*4)
817497 5 (#4)
4X6 IOOHIK *4)
8I792O O <*4)
NO CA1AlVSI
8 I /923 O NONE
4X6 HOBMJ#5•
817927' O (#5)
817931* O < // 5 )
4X6 PUUM<#5)
817935* 3 «//5)
4X6 HUbM<*5)
81794 I O (»5)
817945 O (//5)
4X6 I'DUMI #5 )
817949 3 >
4X6 Clltrj3< //b )
8I8-IU6 O I
8 ia-1 1-1 3 < //G )
8I8G46 3 (//6 )
OX 02
1 O6
1 12
3%
1 13
I 14
57.
118
1 19
07.
1-25
07.
1 27
07.
1 28
2 01
37..
2 O'J
07.
2 O9
2 IO
37.
2 II
2-15
57.
2 17
2 18
07.
2 2-1
2 2'j
37..
:i o i
3 o:>
83
83
02
83
83
O2
83
83
02
83
O2
83
O2
83
83
02
83
O2
83
83
02
83
83
O2
83
83
02
83
83
O2
03
83
56/4
5BO5
5865
5912
5966
6017
.O
0
O
O
6
O
SS IO
SSIO
SSIO
SSIO
SSIO
SSIO
4 1 53
< 2 13
28 4
44 .0
812
134 5
9 8
9 8
9 7
IO 2
9 7
96
O
O
O
O
0
0
176
O33
O43
O43
O36
O6 1
3 459
1 644
O OO2
0 036
O OO3
O O2 1
4 1 5 5OO
4 17.695
422 212
4O3 61 1
426 4O4
428 43O
0
0
O
O
O
O
O4 1
OO5
263
243
237
26O
N/A
O
O
O
O
O
02O
O27
025
oia
O46
O 5 1 7
N/A
N/A
N/A
N/A
N/A
AGAIN
6O66
61 16
6 168
6222
6277
6425
6477
6533
6587
6685
674 1
687 1
6927
6997
7047
O
O
0
O
O
O
O
.O
O
O
0
.0
2
.0
7
SSIO
SSIO
SSIO
SSIO
SSIO
SSIO
SS IO
SSIO
SSIO
SSIO
SSlO
SS IO
SS IO
SSIO
SSIO
35 05
226 62
N/A
N/A
N/A
69 3
82 O5
- 1 O
- 1 O
N/A
N/A
N/A
N/A
N/A
N/A
97
N/A
N/A
N/A
IO 1
IO 3
N/A
N/A
IO. 1
9 9
10 1
IO 1
IO 1
IO O
10 1
O
O
0
O
O
O
O
O
O
O
O
O.
O
O.
O.
1O3
6O2
392
485
372
3O3
261
287
376
549
531
67 1
628
575
543
3 569
13 445
8 O7O
8 279
8 784
5 398
4 916
5 OIB
5 286
9 753
8 4O5
7 989'
7 625
7 676
8 652
417 534
N/A
N/A
N/A
392 57 1
39O 249
N/A
. - 1 O
398 IO
398 331
394 56O
391 295
393. 257
397 248
393 277
O
O
O
0
O
O
0
O
O
O
O
O
O
O
0
030
3OO
282
285
293
286
296
286
323
341
329
3O8
305
3OI
293
O
O
O
O
O
0
O
O
O
O
0
O
0.
0
O.
O9O
591
381
475
362
292
249
271
362
534
517
656
615
565
53O
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
-------
4X6
8 I865O
818654
4X6-
B 18662
8 18666
8 18723
4X6
818727
8 IB73I
4X6
8 187 35
8 18739
8 18976
4X6-
8 18992
818996
4X6
8 19243
8 19247
CU833I06)
5 ( //6 )
5 (#6»
2OHl)( H'l )
O ( // 7 )
O (*7)
0 (*7)
20POU7)
3 <*7)
3 (X/7)
2OHD( #7 )
5 (*7)
5 <«7)
5 <*7>
AG( *BI
O (08)
o (//a)
AG( #8)
3 <*8)
3 (#8)
by.
:i ou
3 O4
ox.
J IU
3 1 1
3 IS
3'X.
3 16
3- 17
S%
3 ia
3 22
3 23
0%
4 O7
4-O8
3%
421
4 22
02
B3
83
02
83
83
83
O2
83
83
O2
-83
- 83
83
02
83
83
O2
83
83
7 104
7 156
7288
7345
7396
74S2
7504
7561
761 1
7663
797 1
8O23
8254
8326
6
.O
7
O
O
0
0
O
O
O
O
O
O
8
SSIO
SSIO
ss 10
SSIO
SSIO
SSIO
SSIO
SSIO
SSIO
SSIO
SSIO
SSIO
SSIO
SSIO
N/A
N/A
N/A
N/A
N/A
N/A
N/A
- 1 .O
- 1 O
- 1 O
N/A
- 1 .O
- 1 O
- 1 0
9
to
IO
10
10
IO
IO
IO
IO
9
IO
9
9
10
9
1
1
1
1
O
1
1
1
9
2
9
8
1
O
0
O
0
o
o
o
o
o
o
o
o
o
o
6O8
677
2OO
265
O39
O74
071
112
IO9
IO6
29O
197
548
216
8 O84
a 208
2 OI4
2 429
2213
O O2 1
O O35
O O66
o oie
0 O51
6 839
6.491
9 261
9 601
4OI 134
394.334
4O2 2IO
402 88O
4O3 175
4 13 O2 1
4O7 28 1
4O5 92
4O5 27
4 14 168
391 652
4O3 087
4OI 849
39O 667
0 307
O 322
O 045
O O46
O 010
O 279
O 28 1
O 27 1
O 276
O 275
O 298
O 292
O 367
O 251
O
O
O
o
o
O
0
O
593
665
187
249
O23
O58
O58
O963
N/A
N/A
O
O
o
o
28O
1838
5347
2160
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
-------
NUMBER 02 CAI//
DAI t
UUOM I PRO
AI.OY
MPG
MC
SIOCK Cfl 1 Al YSI
8 112 14 9 SIOCK
8 142 17 9 SIOCK
814220 9 SIOCK
814223 9 SIOCK
NO CAI A! YSI
8 15242 O NONE
8 15244 O NONE
8 15246 O NONE
NO C A I A L Y S 1
8 15252 3 NONE
8 15257 3 NONE
815258 3 NONE
NO CA 1 Al YSI
8 15266 5 NONE
8 15268 5 NONE
8 !527Ot 5 NONE
4X6 12 : 1 ( * 1 )
8 I6O32 0 ( // 1 )
815994 O ( H 1 )
4X6 12 : II // I )
8 I6OO2 3 (//It
4X6 12 : l( // 1 )
8 1 GOOB 5 < tt 1 )
8 I6O1O 5 < # 1 >
4X6- 12 : K It I )
8 I6OI7 3 (» 1 t
8 I6OI9 3 (// 1 )
NO CAI Al YSI
8I6O25 O NONE
6 X K 1 O 12. 1 1 // 2 )
816563 0
6XK IO 12 : l( //2 )
H I657H 5 ( «2 )
(116582" !j (//2)
b 2y
6 30
7 Ol
7 02
OZ
8 13
8 17
B 17
J'X.
8 20
a 25
8 26
5%
9 IO
9 IO
9 1-1
0%
9 16
9 2 1
3%
9 29
57,
IO Ol
10 Ol
37..
IO OB
to oa
0%
10 II
oy..
IO 19
1 1 O2
sy.
1 1 O'.i
1 1 IB
82
02
82
82
02
82
82
82
02
82
82
82
O2
82
82
82
02
82
82
02
82
02
82
82
02
82
82
O2
82
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8 19248
l'UHM(0t> I
. 3 <05|
3 (05)
l'imM(//'a)
5 I>|*7I
5 <»/)
5 (*7I
5 ( // / I
A(.( VB I
O ( 08 )
0 ( '/B )
- A(i( 08 )
:i (0a>
3 ( 08 )
-j
2
•j
'2
•2
2
;j
3
3
3
3
3
3
3
3
:j
3
3
4
•1
•1
4
J'X. 02
1 1 83
Ib 83
b/i. 02
17 83
IB 83
()•/. O2
24 83
25 83
3"/. O2
Ol 83
O2 83
b% 02
03 83
O4 83
O% 02 •
IO 83
1 1 83
15 83
3% O2
16 83
17 83
57. 02
IB 83
22 83
23 83
0% O2
O7 83
08 83
37. 02
21 83
22 83
6535
6591
668B
6743
6874
693O
7OOO
7O53
7 IO8
7 159
7294
7348
7399
7454
75O6
7563
7614
7666
7974
8O26
8259
8392
O
.O
O
O
0
0
O
2
a
1
7
O
0
o
o
o
o
o
8
O
O
o
SS30
SS3O
SS3O
SS30
SS3O
SS3O
SS30
SS30
SS3O
SS30
SS30
SS30
SS30
SS3O
SS30
SS3O
SS30
SS30
SS30
SS30
SS3O
SS30
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
- 1 O
N/A
- 1 0
- 1 O
- 1 O
N/A
212
2O 9
215
212
20 9
21 O
20 a
21 3
2O 5
20 a
2O 7
20.9
214
21 O
21 4
21 1
21 O
219
2O 9
219
22 O
O 125
O 137
O 258
0 252
O 394
O 4O3
O 408
0 412
O 288
0.375
O OI8
O OI2
O 009
O OO9
O 008
O OO9
O O09
O OO9
O 221
O 233
0 134
O. 12 1
3 246
3 977
4 576
4 47O
4 87 1
5 220
4 342
5 O56
3 456
4 37O
1 332
O 862
1 184
-O OO4
O.OO7
O Ol 1
O OO6
- OO4
4 O90
4 086
4 383
4.898
1 0
187.662
188 833
184 O26
IBS 177
187 372
188 OI3
189 016
186 539
192 543
195 359
197 413
195 432
192 BOO
195 931
192 34
195 22
196 370
I8O 868
189 955
181 073
178 946
1 OS/
1 O67
1 O94
1 056
1 1 13
1 1 19
1 107
1 1 19
O 816
1 1 13
O OI5
O O3O
0 010
1 OIB
1 012
1 OI8
1 O74
1 III
O 971
1 108
O 967
O 9O8
O. 122
0. 132
0 254
O 247
O 39O
O 397
O.4O5
O 4O8
O 285
O 368
O OI3
O.OO7
O O04
O OO5
0 OO4
O OOS
N/A
N/A
O.2I7
O 2287
O 1295
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
I
ro
o
-------
NIIMUtU 02 CAIv
HAIL
UIJOM IPIIU
AIOY
MI'li
IIC
CO
CO 2
NOX HC-NM
ME (HANOI
SMH.K CA I Al VSI
8M2I5 Li SIOCK
8 1-12 IH 9 SIOI.K
a 1-122 I 9 SIOCK
814224 9 SIOCK
NO CAIAl VSI
6 1524Ji O NONE
B 15245 O NONt
8 152-17 O NONt
NO CAIAlYSI
a 15253 3 NONE
8 15256 3 NONE
8 15259 3 NONE
NO CAIAt YSI
a 15267 5 NONE
a 15269 5 NONE
8 1527 I 5 NONE
()
6
i
/
a
a
u
a
a
a
u
9
u
'29
HO
Ol
02
0%
13
17
17
3"/.
2O-
25-
26
5V.
IO
IO
l-l
U2
82
82
82
02
82
82
82
02
82
82
82
02
82
82
82
2685
2739
28 IO
28bO
3192
3213
3235
334O
3396
3425
3595
3625
3662
O
4
O
.O
O
0
O
O
O
O
5
O
0
SS4O
SS40
SS4O
SS40
SS4O
SS40
SS40
SS4O
SS40
SS40
SS40
SS40
SS40
O
0
O
0
197
170
166
ISO
5
OO
64
54
7
5
3
9
N/A
119
113
1 17
1 19
9
5
4
6
2 1
2O
2O
2O
18
21
19
2O
20
19
19
20
2O
b
O
. a
a
7
6
5
6
1
a
4
0
2
O
O
O
O
O
O
O
0
O
O
O
O
0
OO2
.002
GO)
OO3
381
309
329
29O
289
299
307
283
291
O UI6 191 641 O O32 O OO2 O OO2
O O 206 162 O 256 O.OOO O OO I
O O2B 198 O55 O O55 O.OO2 O OOI
O.O36 198 112 O OI5 O OO3 O.OO2
4 229 212 537 I 843 O 381 I O24
3 813 183 906 I 583 O.3O8 O.722
4 O76 2O3 I9O I 698 O 328 O 926
4 245 192 367 I 6OI O.289 O 774
4 O82 197 967 I 693 N/A O 828
3 865 2OI 364 I 639 N/A O 947
3 895 2OS 590 I 761 N/A O 789
3 969 198 963 I 695 N/A O 743
4 O74 196 239 I 627 N/A O 89 I
I
ro
-------
APPENDIX 5
Statistics with the Data
Stratiriea by Oxygen Level,
Test Cycle, and Individual Catalyst
-------
NUM>t{..
lit
b»blEM
AU173I
I7JOJJOI EOT
1UE H*Y 10/83
PMUJECTl SAMV
A| 1/:U3:01 rut MAY JO/83
AI 17:03:03 IUE HAY 10/H3
6660660066
60f.6O6666666
66 66
oo
66
60060066666
6oo6o6r>ub66o
66 66
(»b hb
66 66
660606666666
0660066666
1. INtN I'KlNItl) 1374
l'tb PKlNltl) 48
oimuflnrtbBb odbBbbbbHA 2222222222
bdbildbHItdttuB
db bft
bb dli
ciH bu
BubiibHdb
HMUHUbUd
BH db
bli db
Ud b8
blltlMtiildttiiObB
Ulllldllltddbd
bbU^SbbbSb
SSSSbSSSSSbS
Sb bS
bb
bSS
bSSiibbiS
SbiSbbbbb
SbS
bS
bb bS
SbbibSiSbbbS
bf.SbSbSbSS
BHiibrtHbdddrib
bb bb
Bb 8b
Bb 8U
bbbBAdab
HdHHbbdB
88 bb
BH rib
Bri 8b
bbdbbbbbttbdd
ABBBBBBdbb
NN UN
MM NN
NNNN NN
Nit NN NN
NN NN NN
NN NN NN
NM NN NN
NN NN NN
NN NNNN
NN NNN
NN NN
NN N
222222222222
22 22
22
22
22
22
22
22
22
222222222222
222222222222
HH HH
HH HH
HH HH
HH HH
HH HH
HHHHHnHHHHHH
HHHHHHHHHHHH
HH HH
HH HH
HH HH
HH HH
Hri HH
2222222222
222222222222
22 22
22
22
22
22
22
22
22
222222222222
222222222222
444
4444
44 44
44 44
44 44
<»44444444<«4
<,<,<,44<,<,
-------
5-2
oxY:u«CaT: <»I)»THHUSFTP
VAwIAdLF- N MINIMUM
v.ALUf 3 0.3000
lO.MPC, j 13.sao
11. HC 3 .luuSO
12. CO 3 .41630
1...NO* 3 . u->o7u
16.MET.ANOL 2 .3,,00
OESCHlPTIvE MEASUrtES <*> OXY:j«C
VARIABLE N MINIMUM
9.ALOY 3 12.900
In.MPO 3 13.624
11. nC 3 .11310
12. CO 3 .3132U
14. NU* 3 I.a790
l6.MtT.ANOL 3 .2*100
DESCRIPTIVE MEASURES OAY:3«c
VARIABLE" N MINIMUM
9.ALDY •» 16.900
lO.MPf, 4 n.76«
11. HC •» .10b2U
12. CO t .3^300
14..NOX UAY:U»C
VARIABLE ' N MINIMUM
9.ALOY
-------
5-3
12. CO
14..NOX
16.METHANOL
OESCHIPTIVE MEASURES
VAHU8LE
9.AUOY
IO.MPG
11. HC
12. CO
U.NOX
16.METMANOL
DESCRIPTIVE MEASURES
VARIABLE
9.ALDY
10.MPO
11. MC
12. CO
1<». NO*
16.METMANOL
DESCRIPTIVE M£ASU*tS
VARIABLE
*.ALOY
IO.MPG
11. nC
12. CO
l'...<*0x
16.METHANOL
2
2
1
<:
N
3
3
3
3
3
0
<«
N
1
1
1
1
1
0
<;
N
1
3
3
3
3
0
.70390
.7SS30
.82000
j> OXY:J*CAT
MINIMUM
13.300
13.672
.11*^0
.23500
2.u2<»<:
» OAY!3»rAT
MINIMUM
20. SOU
13.76J
.13130
.43V20
2.y»39
'> OAY:U«CAT
MINIMUM
i-y.sOO
1 3. OHO
. 14620
1.J573
.a3v3o
.a<»03U .77210
.7672U .76125
.32000 .82000
: (i» -1
.d^Uo .2
STO OEV
.v863d
.00625 -1
.76d<*6 -2
.1*720
.22030 -1
STD OEV
STU OEV
.iia7fc
.7U.*T. -2
.13612
.ISdlO -1
-------
5-4.
V AW I ABLE.
9.ALOY
10.MPG
11. HC
12. CO
14.NOX
16.METHANOL
OcSC»IPTIVE MEASURES
VA9IA8LE
9.ALOY
10.MPG
11. HC
12. CO
U.NOX
lo.METMANOL
DESCRIPTIVE .-EASUHES
VARIABLE
9.ALOY
10.MPG
11. HC
12. CO
14.NOX
Ifr.METHANOL
3E5CSIPTIVE MEASURES
VAMIA8LS
9.ALDY
10. MHO
11. HC
12. CO
N
1
2
2
2
2
2
<••
N
2
2
2
2
2
*
<;
N
3
3
3
3
3
2
< ]
N
2
*
2
2
MINIMUM
72.900
13.365
.13660
.3*530
<:.03l7
.2UOo
»> OXY:b»CAT
MINIMUM
117»3u
13.*85
.13100
.34V90
1 .V74j
.2,600
lo> OAY:O»CA
MINIMUM
38.550
13.4li
.15330
1.3873
.72610
.3J900
.!> OxY:3<»CA
MINIMUM
39.330
13.3&7
.13640
.J057U
MAXIMUM
72.900
13.4VO
.16360
.35530
2.0833
.3,000
: (»3) »TP«o
MAXIMUM
117.40
13.530
.19940
.44060
2.092V
.4,300
T: <»4)»TP*
MAXIMUM
46.900
13.552
.1*020
2.2S67
.73400
.J5200
T : ( »4> «TPKI
MAXIMUM
76.650
U.4^3
.13 1-0
.39360
MEAN "
/2.900
13.430
. leolO
.35030
c.0686
.27600
:FTP
~»f A N.
117. 3b
13.511
.19020
.39525
2.0336
.35950
OSKTP
MtAN
••1.5*7
13.^70
.16VC3
1.9869
.74293
.3«5:50
J'.rfP '
MEAN
07.990
13.431
.144*0
.3;vbb
sru'uEv
.V2702
.49497
.70711
.23900
.,031U
STD OEV
.70711
.37547
.13011
.64133
.83863
.39403
STO OEV
4.6472
.73140
.19041
.35*95
.14981
.,1924
STD OEV
12.2*7
.V0722
.VIV24
.19723
- 1
-1
-2
-2
-1
-1
-1
-1
-1
-1
-1
~l
-1
-1
-1
-2
-1
-2
-1
-------
5-5
14.NOX
16.METHANOL
OESCHIPTIVE MEASUHES
VAHIABLE
9.ALOY
lO.MPG
11. MC
12. CO
1<*.NOX
16.METHANOL
DESCRIPTIVE "EASUHtS
VARIABLE
9.ALOY
10.MPG
11. HC
12. CO
1».NOX
16.METMANOL
OESCHIPTIVE MEASUHES
VARIABLE
9.ALOY
1 0 . MPG
11. MC
12. CO
14.NOX
16.METHANOL
OESCHIPTIVE "EASiMEs
VARIABLE
2 1.9570 2.00d2
0
<12> OxY!3»CAT: <»4) «TPi
N MINIMUM MAAlMUrt
3 111.2V I72.e7
3 13.227 U.32*
3 .IslOu .175*0
3 .2ae*0 .4b78u
3 i.Vb32 2.10VO
0
OXY:O»CAT: (»?)*TP
N MINIMUM MAXIMUM
2 118.46 119,24
1 U.141 14.141
'i .2767u .27700
2 i.^32 2.V7UO
2 1.9502 1.9934
u
<14> UXY: j»CAT: (»b) oyM1
N MINIMUM MAXIMUM
2 117.52 1-1.23
11T W^W IT 2U«i
1 J . O73 1 J • 3T3
2 .27<*9o . OXY:i«CAT: (»5) •TP'
N MINIMUM MAXfTjM
1.9826 .36204
*0 : K TD
MEAN STu OEV
I4l.d7 30.691
13.2^4 .52472
.15983 .13522
.35630 .o9B59
c.0516 .db'o34
W.t TP
MEAN STO OEV
U8.85 .55154
14.141
.27685 .21213
d.ablO .18074
1.9718 .30547
HO:FTP
M£AN STD OEV-
12V. 37 le.766
1 T 3 AU.
13 .393
.27800 .O341
-------
5-6
9.ALDY 3 13* !.**** 1.9378
IB.METHANOL 0
DESCRIPTIVE MEASURES OAY : u»CAT: (*6> »TPRQ:r TP
VARIABLE N MINIMUM MAAlMUM MEAN
V.ALDY • 2 OXY : J«CAT : ( i»6) »TP«u:FTP
VAWIA8LE N MINIMUM MAAlMUM MtaN
9.AUCY 2 JU.4/ 332.13 322.31
10.MPG 2 13.433 1J.44* 13.441
11. HC 2 .8B460 .^2010 .^0235
12. CO 2 7.^14J 7.3714 ?.2928
U.NOX 2 I.al47_ Ual97 1.^172
Ib.METHANOL 0
DESCRIPTIVE MEASURES OXY :^«C4T : ( *M 2JPSO IP "=.
VAWIASL£ N MINIMUM MAAI.MUM '-I£AN
Q.ALOY t. J04.13 J2<».3i jij.37
10.MPC 2 13.-»33 !3.bJ6 13.471
ll.nC 'e. .^3240 .V0550 .a68y3
12. CO 2 o.ae2B b.^bjs 0.9331
14.NUX £. i.0133 1.6320 1.62^7
23.757
.09851
.71319
.28616
.20936
STD OEV
32.67S.
.43275
.32527
.28991
.28001
STO OEV
13.916
.11243
.25102
.11109
.35355
STO OEV
13.189
.50134
.316*0
.71206
.13081
-1
-2
-1
-1
-2
-1
-1
-1
-2
-1
-1
-1
-1
-------
5-7
16.METMANOL 0
OESCHIPTIVE MEASUKtS <19> UXY:0«C*T:(*7>
N MINIMUM MAXIMUM
J JS.3bo 4o.6JO
3 i3.6d<: U.91b
.iOOdO
i.09^3
.70290
MEAN
9.ALUY
10.MPG
ll.riC
12.CO
14.NOX
Ib.METMANOL
3 .16600
3 1.4919
3 .62510
u
13.810
.18483
1.B392
.36630
OtSCWIPTlVE MEASURES <2u> OXY:3»CAT:(»7)*TPHOJFTP
VARIABLE N MINIMUM MAXIMUM MEAN
9.ALDY
IO.MPG
11. «C
12.CO
U.NOX
16.METMANOL
i bd.67C
2 13.766
2 .1<»590
2
99.720
13.90U
.^•0400
1.9360
^4.195
13.833
.15235
.39905
1.8955
OESCHIPTIVE MEASURES
VAPIA8LE
9.ALOY
OXY :u»CAT: (»8) *TPHU:FTP
** ,* *
MINIMUM MAXIMUM MtAN
3 »»l.aOO 66.040 3S.4J3
STU OEV
.17094 -l
.Jl166
.39103 -1
STO OEV
7.3135
.96288 -2
.70004 -2
.60104 -1
iTU OEV
-------
5-8
10.MPG 4 13.76b 14.03e 13.853
ll.HC 4 .4«»600 .61130 .53958
12. CO 4 0.2V19 6.6857 6.5252
14.NOX * 2.U08J 2«u506 i.02M2
16.METHANOL 0
DESCRIPTIVE MEASURES <23> OXY:3»C*T: twqj «TP-*0:FTP
VAHIA8LE N MINIMUM MAAlMJH MEAN
9.ALDY 0
10.MPG 3 '13.601 13.877 13.709
ll.HC 3 .3a26e .478ii .42799
12. CO 3 5.473b a.4773 b.9313
l<».MOx 3 1.977b 2.U06^ 1.9892
16.HETHANOL - 0
DESCRIPTIVE MEASURES <<:4> jXY:a«CAT: (»8) »TMHu:FTP
VAPIA8LE N MINIMUM MAXIMUM M£AN
9.ALOY 0
10.MPG 1 13.786 U.7oo 13.786
ll.rtC 1 .54175 .541/s .34175
12> CO 1 6.V62U 6.^620 0.9620
U.NOX 1 1.391V 1.0919 1.8919
16.METH&NOL 0
DESCRIPTIVE -ASUKE, <^> OXY : ,-CAT :^t-TH,u:, :P
vAKiASLS N MINIMUM MAAI^UM ^EAN
V.ALOY 11 I3i.6u 3^5. 7/i £4l.b9
10.HPG 13 13.39V 14.172 13.386
ll.rtC 14 .70480 1.U563 .91903
12. CO 14 7.1*22 3.4^i V.3196
14.NOX !«. l.,«,5o 2.^00^ <.Ud32
le.METHANOL 4 1.7a30 2.4530 £.1767
.12764
.68705 -1
.16906
.18448 -1
STO OEV
.14700
.66416 -1
.50769
.14357 -1
STD OEV
5Ti) UEV
30.265
.24U9
.36235 -1
.J912U
.9012b -1
.2dl97
-------
5-9
DESCH1PTIVE MEASUHtS
VARIABLE
9.ALOY
IO.MPG
11. MC
12. CO
14.NUX
llS.METHANOL
DESCRIPTIVE MEASUKES
VARIABLE
9.ALDY
IO.MPG
11. nc
12. CO
14.NOX
16.M&THANOL
DESCRIPTIVE MEASUKES
VARIABLE
9.ALOY
10.MMG
11. HC
12. CO
14. NO"
Ib.MiTHANOL
N
3
3
3
5
5
3
N
4
6
6
6
6
3
N
i»
6
b
b
o
u
io> UXY:
MINIMUM
252.60
13.686
.7a950
7. 1572
£.0030
i.uiao
!7> OXY:
MINIMUM
1&5.00
13.464
.7675*
7.0UU
1.9903
,.4130
'.H> OXY:
MINIMUM
17.200
13.922
. U560
.69,70
• 5 3 0 4 OXY:J«C4T:iTOCK»TPHO:rTP
VABIA8LE N MINIMUM MAXIMUM M£AN
-------
5-10
12
14
16
.CO
.NOX
.METHflNOL
otscHiPTivE MEASURES
9
10
ii
12
14
16
VAHU81.E
.ALDY
. MPR
.r(C
.CO
.NOX
.METHANOL
1
1
1
•
1
•
N
.3
60340
.9496
5o70o
OXY:
MINIMUM
•
30000
J 17.219
3
3
3
2
•
30000
.<2e9uo
.
.
54040
60000
•
1
•
o»r.aT:
60340
.9496
bb70o
.60340
1.9496
.56700
<»M •TPSQtH'.Y
MAXIMUM
1
1
•2 .
-1 .
•
-2 .
.0000
7.4J9
>»1000 -2
64000 -1
63290
12000 -1
MEAN
.53333
17.318
.33667 -2
.48300 -1
.61050
.90000 -2
STO OEV
.40415
.11160
.03509
.19196
.27084
.42426
-3
-1
-1
-2
OESCHIPTlvE MtASUKES O2> OXY : 3»CAT : (»1 ) »TPHO:PMY...
9
10
11
12
14
VARIABLE
.ALDY
.MPG
• HC
.CO
.NOX
16.METHANOL
OESCHIPTIVE MEASURES
9
10
11
12
14,
VAPIA8UE
.ALOY
N
3
3
3
3
3
3
MINIMUM
1
.0000
17. OBI
•
0
2
•
<3J>
N
4
aiooo
•
.4257
40000
MAXIMUM d&Atil
1
.6000
18.712
-2 .
•
2
•2 .
9««000 -e
OSOOO -2
.JS921 !
50000 -4
1.2333
17.745
.86333 -2
.45333 -2
i.7338
.43333 -2
STO OEV
.32146
.85690
.68069
.42782
.26688
.b773i
-3
-2
-3
uxY:b«CAT: OXY :
-------
5-11
VARIABLE
9.ALOY
lO.MPd
ll.nC
12. CO
14.NOX
le.METHANOL
N MINIMUM
3 .30000
3 17. 147
MAXIMUM
1.6000
U.U40
v(d£jlN
1.1667
17.721
STU OEV
.4Q41S
.49843
3 .50000 -2 .12900 -I .U3000 -c .41073 -2
3 .5/200 -1 .6710U -1 .62533 -1 .49943 -2
3 .47^20 .69750 .55043 .12737
2 .40000 -2 .55000 -I .34300 -] .*3134 -1
DESCRIPTIVE M£ASU«ES <35> Ox Y : :i«CAT : ( »2)
VARIABLE N MINIMUM MAXIMUM
9.ALDY
M£4N
ll.HC
12. CO
14.NOX
16.M£TMANOL
>jTu OEV
3 l.oOOO 2.3000 iTo333 .J7859
3 17.295 17.4<»<2 17.368 .73406 -1
3 .82000 -2 .*3000 -e .8733J -2 .55076 -3
3 .2J40U -1 .^7600 -1 .25033 -1 .22502 -2
3 k.d026 2.060<: £.3384 .31270 -1
3 .90000 -2 .23000 -1 .14QOP -1 .78102 -2
OESCHIPTIVE MEASURES <36> UXY :5«CAT : (»2) •
VARIABLE N MINIMUM MAXIMUM
9.ALOY
10.MPR
ll.HC
12. CO
14.NOX
16.METH4NOL
DESCRIPTIVE
VARIABLE
9.ALDY
10.MPG
11. MC
12. CO
M£4,N
1 2.2000 2.20UO 2.2000
1 17.366 17.366 17.366
1 .90000 -2 . VOOOO -2 .S>6000 -2
1 .28200 -1 .2b200 -1 .2o2uO -1
1 c. 7982 2.79a2 Ox Y : 0«CAT : ( »3 )
N MINIMUM MAXIMUM w£4N STQ OEV
1 .91000 .*1000 .vlOOO
3 1ft. -919 17.34** I7.1b5 .21603
3 .01000 -2 .90000 -2 .73333 V2 .14i*7B -2
3 .1^850 .2312U .216J7 .16560 -1
-------
5-12
14.NOX
16.METHANOU
3 .62550
0
.6478U
.63983
.12439 -1
DESCRIPTIVE MEASURES UXY:3»CAT:<*3)«TPRO:nWY
VARIA9LE
9.AUDY
10.MP6
11.MC
12.CO
16.METHANOL
N MINIMUM" — MAA1MUM MtAIT iTD OEV
1 1.7000 1.7000 1.7000
.3 16.40J 17.07V 16.Vi8 .14392
3 .95000 -2 .10000 -1 .98000 -i .26458 -3
3 .60000 -3 ,17^0y -1 '.o2000 -2 .Vo99b -2
3 sl.739e 2.0118 i.7&95 .J7842 -I
2 .11000 -1 .16000 -1 .13500 -1 .J33SS -2
DESCRIPTIVE MEASURES <3s»> OXY:S*CAT: (»3) *TPHO:nwT
VAHIA8LE N MINIMUM MAXIMUM MtAN STU UEV
v.ALOY JXY:O«CAT:t»4)«TPKO:MWY
VARIABLE N MINIMUM MAXIMUM
9.ALOY
11.HC
12.CO
14.NOX
16.METHANOL
DESCRIPTIVE MEASURES <4i>
VAHIA8LE N MINIMUM
STu DEV
3 .36000 1.1000 .7233J .J7018
3 16.909 17.04- 16.976 ..67453 -1
3 .*JOOO -2 .64QOu -2 .55000 -J .10817 -2
J .2va«0 ,J45bO .3262'J .24j81 -1
.507^.7
.30000 -2 .
-------
5-13
9
10
11
12
14
16
.ALOY
.MPO
.HC
.CO
.NOX
.METHANOL
2
2
2
2
2
0
DESCRIPTIVE *£ASUHtS <'
9
10
11
12
U
16
OESC
9
10
11
12
14
lh
VARIABLE
.ALOY
.MPG
.HC
.CO
.NOX
.METHANOL
XIPTIVE M£asuntS
VARIABLE
.ALDr
.MPG
.HC
.CO
.NO.
.M£THANOL
N
2
2
2
2
*
i)
o
N
2
1
2
2
2
0
1.6700
17.010
.73000
.86000
i.646V
•2> UAY:
MINIMUM
2.0500
1
1
-2 .
-2 .
2
3*CAT:
.vooo
7.oai
SiOOOo -(.
14400 -1
.0516
(»4> »TPk(j
MAXIMUM
2
.aOOO
16.940 17.061
.aoOOO
. 10700
2./164
0> UXY:
-2 .
-1 .
" 2
0»CAT:
V4QOO -2
14500 -1
.7267
(»5)»TPRO
1.7850
17.046
.61500 -2
-11500 -1
^.6492
:hwY
M6.AN
i.7250
17.010
.90000 -2
.12600 -1
•i.7215
:nwY .
MlNlMOM* MAXIMUM "EaN .
2.6400
17.S8B
.13000
1.3040
1.545*
DESCRIPTIVE MEASUKES <*<•> UAY:
9
10
11
12
14
VARIABLE
.ALOY
.MPG
.HC
.CO
.NOX
N
2
1
2
2
2
MINIMUM
2.7600
17.310
. 13200
.30600
) »TPyu
MAAlMUM
3
1
-1
-L .
2
.2000
7.310
1J200 -i
aOSOo -1
.63oo
J.1150
17. baa
.15300 -1
1.4826
1.63*4
:n«Y
«6lN
^.^00
17.510
.13200 -1
.4570U -1
i.60 15
.16263
.30205
.14021
.-1012
.J3234
STO 06.V
.10607
.V9419
.56569
.26670
.72a32
STu OEV
.67175
.11314
.25180.
.12516
STO OEV
31113
.<;1355
.4
-------
5-14
16*M£THANOU
9.
10.
11.
12.
14.
16.
VARIABLE
ALOY
MPG
HC
CO
NOX
METMANOL
N
2
2
2
2
2
u
OESCHIPTIVE M&ASUKES «
9.
10.
11.
12.
14.
16.
VARIABLE
ALOY
MPG
HC
CO
NOX
METMANOL
N
2
2
2
2
2
0
OESCSIPTIVE MEASUKES °
9.
10.
11.
12.
U.
Ib.
VARIABLE
ALDY
MPr,
HC
CO
NOX
MfcTHANOL
OESCHIPTIVE MEASURES
9.
VAHU6LE
ALDY
N
2
.2
2
2
*
0
MINIMUM MAXIMUM MEAN
ll.*dO 17.400 l4.fc.7U
17.553 17.836 17.695
.1J300 -1 .14600 -1 .13950
.32970 .b0450 .41710
2.6354 2.645P £.6404
*6> OXY:O«CAT: <»6)*TP9o:nwY
MINIMUM MAXIMUM M£4N
12i.ll 136.31 130.71
16.69SI 17.363 17.032
•2017U .34630 .30400
b.d«4^ 6.V963 O.VOS7
i.JVOe 2.429J i.40V9
*7> OXY:3«CAT: «l*i) «TP«U:HWY
MINIMUM MAXIMUM "It UN .
136.34 137.98 i37.16
lo.904 17.020 16.962
.1*410 .20530 .19970
6.J26/ 6.516V 0.421B
2.^573 i.302^ d.2S03
STO OEV
4.228S
.200J9
-1 .91924
.12360
.71418
5TU OtV
7.9196
.47065
.391921
.12099
.27365
STD OEV
1.1597
.d<2J07
.7919o
. 134*9
.31*91
-3
-2
-1
-I
-I
-2
-1
<4«j> uXY :b*CAT : ( »6) •TPt^u JHWY
N
2
MINIMUM MAXIMUM MtAN
12A.33 127.17 124. 2S
STO OEV
4.1295
-------
5-15
10.WPG
11.HC
12.CO
14.NOX
16.HETHANOU
2 16.53ti
c .13080
2 6.0667
2 2.2044
0
10.914 10.726
.16900 .14990
6.2852 0.1759
.26587
.27011 -I
.1543'U
-2
DESCRIPTIVE "EASuKtS -<4-y> UXY:u*CAT : ( »7)
VAWIA8I.E N MINIMUM MAXIMUM
2 1.S700 1.9900
9.AUOY
10.MPG
11.HC
12.CO
14.NQX
16.METHANOL
M£iN STD OEV
i.^300 .o48S3 -1
3 17.107 17.39 OXY:3«CAT : (»7) «TPRO:nWY
VAHIABLt
STD
ll.rtC
12.CO
14.NOX
16.METHANOL
MINIMUM MAXIMUM MtflN
2 i.4400 2.V300 i.ftSSO
2 17.010 17.0 UXY:S«CAT:l»7)
VARIABLE . N MINIMUM MAXIMUM
9.ALDY
10
11 .HC
12. CO
16.HETHANOL
MEAN STU DEV
3 2.3bOu 3.3^00 2.9000 .30567
3 16.b7i 17.150 17.034 .14526
3 .7VOOO -2 .10530 -1 .89500 -2 .14080 -2
3 .bOOOu -3 .'.lOOO -d .23000 -2 .1997s -2
3 i.bllo 2.72b'«»
-------
5-16
DESCRIPTIVE MgASUHtS OXY:0»CAT :(»>»)'
VARIABLE N MINIMUM MAXIMUM M&AN
3 1.920U 3.1500 i.3633
3 17.02- 17.IS1* 17.101
3 .20880 -1 .26900 -1 .23937 -
-.363S -.255H
9.ALUY
10.MPG
11. HC
12. CO
14.NOX
16.METHANOL
STO OEV
.68311
3 UXY:3«CAT:<*8)»TPHO:hWY
VAHIABLE N MINIMUM MAXIMUM Mt4N 5TU 0£V
9.ALDY 0
10.MPG
11.HC
12.CO
1<..NOX
16.METMANOL 0
DESCRIPTIVE MEASUHES OXY:5«CAT:f»8)*TH«u: HWY
VARIABLE N MINIMUM MAXIMUM M£AN STU 0£V
0
2 17.513 18.88V 18.201 .47263
2 .21340 -1 .2381U -1 .22575 -1 .17<»66 -2
2 3.0J21 5.1001 b.0661
2.5 UXY : u»CAT :,
VARIABLE N MINIMUM MAXIMUM
9.ALOY 12 69.130 215. U
10.MPG 13 Ib.o3<5» 17.502
U.HC 1-
MEAN STD OEV
i68.2iS 3^.0^
17. i^ .27712
-------
5-17
12. CO
14.NOX
l6.Mfc"THANOL
DESCRIPTIVE i-EASUKES
VARIABLE
9.ALDY
10.MPG
11. 1C
12. CO
14.NOX
16.METHANOL
OESCHIPTIVE MEASURES
VA«IABLE
9.ALDY
10.MPG
11. 1C
12. CO
14.NOX
16.METHANOL
DESCRIPTIVE MEASURES
VAPIABLE
9.ALOY
10 .HPG
11. HC
12. CO
14.NOX
1*.M£THANOL
1* 6.1530
14 OXY:3
N MINIMUM
3 171. 7U
5 17.081
5 .36230
5 3.7837
5 2.0643
3 .BbSOO
OXY:S
N MINIMUM
4 13V. SO
0 17.030
6 .3J43U
6 3.94V9
6 i./45»
3 .79&00
OXY:O
N MINIMUM
•» 0.
4 17.V6-*
4 .eoOOO
4 .00700
4 .40500
4 .20000
7.0037
3.024d
.S»180U
i»CAT:NONi;»TPRO:
MAXIMUM
179.oO
17.526
.•*70oo
6.7fi7i
2.^541
.94800
«CAT:NON£»TPRU:
MAXIMUM
147.00
17.52b
.47930
6.dO="J
2.V44J
.^3700
•CAT:STQCi<»TPHO
MAXIMUM
. 70000
ls.201
-3 .-0000 -2
-1 .15070
-1 .U32U
-2 .70000 -2
0.6671
1.8141
.69280
n*Y
M6.AN
174. SO
17.J40
.4g71(j
0.2162
.11055
• OlHiib' -1
.37500 -H
.32974
.13327
.30907
STU OEV
4.423d
.18174
.33306
.<*404S
.10315
.J407b
STO OEV
J.S656
.19503
.04600
.32737
.3S37J
.71075
STO OEV
. J2ol6
. 10120
. 1560>»
.34^74
.»U2b
.«:2174
-1
•1
-1
-1
-1
-2
"I
-I
-2
"ENSURES UXY : o»OT : ( « I) *TP*u: IOL£
-------
5-18
N MINIMUM MAXIMUM MEAN 5TO DEV
2 .3UOOO -1 .«»OOOU -1 .JbOOO -1 .70711 -a
2 12^.OU 137.Ou 133.00 5.6369
2 .11UOU -4. .<»50vJU -2 .2BOOO -2 .*<*<)** -2
2 0. 0. 0.
2 .3*000 -2 .J^OUO -c ,J*000 -2
2 .<»JOOO -2 .7bOOu -i .60500 -2 , OXY:3»CAT:(*1)»TP»u:IDLE
VARIABLE N MINIMUM MAXIMUM MtAN STU OEV
9.ALOY 2 .2BOOO .3700U .32500 .636^0 -1
10.MPG • 3 125.00 134.00 130.67 <*.9329
11.HC 3 .22000 -2 .26600 -1 .10733 -1 .1375* -1
12.CO 3 .2800U -2 .171*0 .60200 -1 .96747 -1
U.NOX 3 .U90o -1 .^4800 -1 .17400 -1 .6*715 -a
16.METHANOL 3 .1-»000 -2 .U900 -1 .10000 -1 .74719 -2
DESCRIPTIVE MEASURES <63> UXY :s«CAT : ( * 1) «TpP.0:10L£
9
10
11
12
U
16
VARIABLE
.ALDY
.MPG
.HC
.CO
.NOX
.METHANOL
N
3
3
3
3
3
2
MINIMUM
.73000
114.00
.21000 -2
U.
.dlOOO -2
.21000 -2
MAXIMUM
1
.3300
130. OU
•
0
.
«
21000 -2
•
1S100 -I
2200U -2
MEAN
.97333
122.00
.21000 -2
u.
.1103J -1
.21SJOO -2
STO OEV
.J1214
0.0000
.J635U
.70711
-2
-4
CESC^I?T:VE MEASURES <&<•>
VARIABLE N MINIMUM MAAlMUM «£4N STU 0£V
9.ALDY 2 .4500U 1.3*0u .rt9'iOO .62*33
10.MPG 2 13^.0u U6.00 UO.OO a.-653
11.1C 2 .20000 -2 .JOOOU -
-------
5-19
U.NOX
16.METHANOL
2 .53000 -2 .16900 -1 .11100 -1 .b202«» -2
1 .12600 -1 .12600 -1 .12600 -1
DESCRIPTIVE MEASURES UXY:b«CAT: 1*2)»TPRO:IDLE
VARIABLE N MINIMUM MAXIMUM M£AN
STO UEV
9.ALDY
10.MPG
ll.rtC
12.CO
14.NOX
16.METHANOL
1 1.9200 1.&200 1.5200
1 11*.GO 11*.00 11*.00
1 .37000 -2 .37000 -2 .37000 -?
1 .50000 -2 .5600U -2 .56000 -Z
1 .23100 -1 .UKES UAY : 0»CAT : t»»3J «TPkU: IDLE
VARIABLE N MINIMUM MAXIMUM M£AN
STD OEV
9.ALDY
10.MMG
ll.rtC
12.CO
U.NOX
l&.METHANOL
134.00
134.00
133.00
d. .2/000 -2 .^rOOO -i .37000 -«i .1<»U2 -2
2 .30000 -3 .27000 -2 .15000 -2 .16*71 -2
2 .3*000 -2 .93000 -2 .72500 -2 . OXYt3»CAT:(«3!*TPfrO:10LE
VARIASL'E N MINIMUM MAAl«'JM MEAN
STD DEV
9.ALDY
10.MPG
11.1C
12.CO
1U.NOX
16.METHANOL
1 10.380 10.330 10.310
3 IU.00 U«».OU H7.00 o.2<»50 .
3 .SdOOO -2 .71500 -1 .32167 -1 ,J<.71& -1
3 .10000 -3 .i7l20 .10*10 .1^31»
3 .2370U -1 .32900 -1 .27067 -1 .30713 -2
1 .3*200 -1 .3-.200 -1 .3*200 -1
DESCRIPTIVE MEASURES <6*> OXY:^«C4T:(»3)•Tf*ut 1UL?
VARIABLE N MINIMUM MAXIMUM M£4N STO OEV
-------
5-20
9.ALOY
10.MPG
11.MC
12.CO
14.NOX
Ib.METHANOL
DESCRIPTIVE
VARIABLE
9.ALOY
2 49.640 56.2oO S2.950 ».6alO
2 111.00 121.00 116.00 7.0711
'<. .35900 -1 .70900 -1 .53400 -1 .2474* -1
2 .29000 -2 .b6000 -i .42500 -2 .19092 -2
2 .1410U -1 .18900 -1 .16450 -1 .33234 -2
11.HC
12.CO
U.NOX
16.METHANOL
<70> OXY:O»CAT:
N MINIMUM MAXIMUM
3 .43000 14.16U
3 11*.OU Ul.OO
3 .2-*OOu -2 .13710
3 .29000 -2 '.49310
MEAN
a.7333
119.67
STC UEV
7.«iB7B
1.15*7
.51133 -1 .74671 -I
.16630 .48302
3 .41000 -2 .£4000 -1 .12167 -1 .10*71 -1
1 .43150 ,43i5o .43150
DESCRIPTIVE MEASURES <71> OXY:3*CAT:<*4)«TPPO:IDLE
VARIABLE N MINIMUM MAAlMUM MEAN STQ OEV
9.ALOY
10.MPG
11.MC
12.CO
14.NOX
16.METMANOL
DESCRIPTIVE M
VARIABLE
9.ALDY
'£. 4.0400 11.160
2 123.00 U4.00
2 .44000 -2 .01000 -2
7.6000 5.0346
123.50 .70711
.62500 -2 .26163 -2
2 .10000 -3 .J1000 -2 .16000 -2 .41213 -2
2 .10*00 -1 .12300 -1 .11550 -1 .10607 -2
0
ll.riC
12.CO
\tt.NQK
<72> OXY:5«CAT:(»4i»TMWO:iOL-
^ MINIMUM MAAlMUM .'lEAN STQ 0£V
2 26.320 29.110
-------
5-21
Ift.METHANOL
DESCRIPTIVE MEASURES <73> OXY:0«CAT:<»S)*TP*o:iOLE
VAPIA8LE
9.ALOY
10.MPG
11. MC
12. CO
14. NOX
l6.MtTMANOL
OfcSCMlPTIvE MEASURES
VAWIABLE
9.ALOY
lO.MPr,
11. MC
12. CO
Ifa.NOX
16.METHANOL
DESCRIPTIVE MEASURES
VAkUSLE
9.ALDY
10.MPG
11.. MC
12. CO
1 <.. NOX
l&.MtTMANOL
N
2
1
2
2
2
0
<;
N
0
1
2
2
2
0
<;
N
0
2
2
£
2
0
MINIMUM MAXIMUM
13.2fao 13.360
136. Ou U6.00
.80500 -1 .(J9700 -1
.3«sfa8o .fal690
.23100 -1 .2fafaOU -1
'fa> UXY:3»CAT: (i»5)»TP«0:
MINIMUM MAXIMUM
U8.00 120. OU
.99900 -1 .12220
.fau59y . OXY:b»CA;: t»5)*TPHO:
MINIMUM MAXIMUM
lid. 00 123.00
.1J370 .13630
.600«0 .6^200
.faJlOU -1 .'•aeOU -i
M£AN
13.310
i36.00
.85100 -1
. JVOH^
.23750 -1
10L£
MEAN
123.00
.11105
.fa2880
.27150 -1
IDLE
MEAN
120.50
.13510
.621<»5
.fa*»35'J -1
STu OEV
.^8995 -1
.650Sfa -2
.36dfaO -1
.V192'* -3
STD OEV
.15768 -I
.J2385 -1
.JdH91 -2
STO OEV
J.S355
.1V799 -2
.^9062 -1
.i767b -2
OtSCHIPTlvE ME&SURES <7o> Ox Y : 0»CAT : < »6 > «TPRO: IDLE
VAHIA8LE N MINIMUM
9.AL0Y o
STu U£V
-------
5-22
10.MMO
11. MC
12. CO
1*.NOX
Ib.METMANOL
DESCRIPTIVE MEASUHiS
VARIABLE
9.ALOY
1 0 . MPG
11. HC
12. CO
14.NOX
16.METHANOL
DESCRIPTIVE MEASURES
VARIABLE
9.ALOY
10.MPG
H.HC
12. CO
14.NQX
Ift.METMANOL
DESCRIPTIVE MEASUKES
VARIABLE
9.ALOY
10.MPG
11. MC
12. CO
14.NOX
lf>.M£THANOL
2
2
2
2
0
124.00
.14360
.53540
.26200
<77> UXY:
N
0
2
2
2
2
0
<
N
0
2
2
2
2
0
<
N
0
3
3
3
3
0
MINIMUM
lltt.OO
.14010
.5*070
.26*00
7d> OXY:
MINIMUM
112.00
.1=660
.57110
.2i>eOo
79> OXY:
MINIMUM
109.00
.13000
.67700
.iOOOO
U7.00
.14730
.62540
-1 .32900 -I
j»CAT: (**>} *TPPO
MAXIMUM
ui.oo
.10110
.82020
-1 .27900 -1
S«CAT : («6) »TP«U
MAXIMUM
lib. 00
.170&U
.67*60
-1 ,i0200 -1
0«CAT : ( »7 ) »TPi*u
Max I v«(jrf
127.00
-2 .76600 -1
-I .^2<0o
-3 .U700 -1
125.50
.14545
• ic*0^*0
• ^9b50 * 1
:IOLE
-SAN
119.50
.15060
.70545
.27150 -1
SIDLE
MEAN
115.00
.Ie355
.02283
.29900 -1
• IDLE
MfciN
120.00
.35100 -1
.1 J8*3
.67(100 -2
1.1213
.26163 -2
.03640 -1
.4737e -2
STU OEV
2.1213
.140*9 -1
.16228
.10607 -2
STO OEV
4.2426
.*«288 -2
.73iae -1
.*2*26 -3
3TO OEV
9.6*37
.3816B -1
.793J59 -1
.3*306 -2
-------
5-23
DESCRIPTIVE MEASURES 00> OXY:J»CAT: d»7>«TPRu:lDL£
VAHIA8LE N MINIMUM MAXIMUM *EAN STU OEV
0
2 12*.00 12«J.GU 125.00 i.<»U2
2 .73000 -2 .11600 -1 .95500 -2 .28991 -2
2 .23000 -2 .aJOOO -* .53000 -2 .<»2<»26 -2
2 .13500 -1 .2290u -I .19200 -1 .32326 -2
9.ALDY
10.MPG
11. HC
12.CO
U.NOX
16.METHANOL
M6.ASUMES <81> OXY :b»CAT : ( #7) «TP«0: IDLE
VARIABLE
9.ALOY
lO.MPf,
11. HC
12. CO
U.NOX
16.METMANOU
N
1 123.00
2 11V.OO
MAXIMUM
123.00
U3.00
MEAN
123.00
121.00
STU OEV
OXY:u»CAf : (*8) »TPno: IDLE
VARIABLE N MINIMUM MAXIMUM MEAN STU OEV
9.ALOY
11. HC
12. CO
0
2 123.00 U4.0U 147.50 0.36*0
2 .<»150U -1 .66300 -1 .53900 -1 .17536 -1
2 .^5560 .* OXY:3»CAT:(»e)»TPWu:lOLt
VARIABLE N MINIMUM MAXIMUM M£AN STO OEV
9.ALDY 0
lO.MPfi 2 10«».0u 122.00 113.00 l
-------
5-24
12. CO
U.NOX
16.METHANOL
DESCRIPTIVE MEASURES
VARIABLE
9.ALOY
10.MPO
11. HC
12. CO
U.NOX
16.METMANOL
DESCRIPTIVE MEASUHES
VARIABLE
9.ALOY
10.MPG
11. MC
12. CO
U.NOX
16.METMANOL
DESCRIPTIVE M£ASU«tS
VARIABLE
9.ALOY
i o . MPG
11-nC
12. CO
U.NOX
16.METHANOL
* .72220
2 .16*00
0
OXY:
N MINIMUM
•b o.9aOo
7 109.00
3 .ttlSOO
8 .60210
0 .11500
* .Ifl35o
<86> UAY:
N MINIMUM
3 1S.UO
3 12e.OO
3 .73*00
3 .57550
3 .11200
3 .1*0*0
<&7> UXY:
N M I N I MUM
2 19.050
2 i2o.OU
? ,*olOO
'i. .73560
2 .13900
2 .2*560
.8*000
-1 .2*100 -1
O»CAT:NONE»TP&U:
MAXIMUM
2*. 120
l-o. OU
-1 .15910
1.0*70
-1 .*5600 -1
. UXY:o»CAT:STOC^»T^HO:IDLi
-------
5-25
VARIABLE
lO.MPr,
11. HC
12. CO
14.NOX
16.METMANPL
N MINIMUM
4 0.
•» 11*. 00
4 .19000 -2
4 .27000 -2
4 0.
4 .7UOOU -3
MAXIMUM
.13000
124.00
.53000 -2
'.10840
.17000 -2
.21000 -2
MEAN
.85000
119.75
.27000
.29825
.62500
.IbOOO
-1
-2
-1
-3
-2
STD OEV
.38023 -1
*.J49J
.17*93 -2
.32397 -1
•oOV8* "3
• 3 d 6 V a »3
DESCRIPTIVE MEASURES UXY:O«CAT:(»1)•TPHO:bS10
VAWIA8LE N MINIMUM MAXIMUM MEAN STD OEv
2 .2uOOO 1.1*000 l.OSOO 1.2021
2 10.000 10.100 10.050 .70711 -1
9.ALOY
10.MPG
11.HC
12.CO
14.NOX
16.METHANOL
OESCHIPTIVE
VARIABLE
9.ALOY
2 . liOOO -1 .^8000 -1 .20000 -1 .111414 -1
2 U. 0. U.
2 .10000 -1 ,<»5000 -1 .27500 -1 .*«»749 -1
2 .ttUOOO -2 .oOOOO -1 .3<*000 -1 .J6770 -1
STD OEV
S.302H
.1527b
UXY:J»CAT: (»n»TPWO:$Slo
N MINIMUM MAXIMUM MEAN
3 l.JOOO 11.70U 3.9000
3 10.100 10.400 10.267
J .24000 -1 .JdOOO -1 .28000 -1 .07178 -2
3 .16000 -I .J400U -1 .27667 -1 .10116 -1
3 .2o*OU .J010U .29000 .9539* -2
3 .60000 -2 .VOOUO -2 .73333 -2 .lS27b -2
11. HC
12.CO
U.NOX
1<).METHANOL
DESCRIPTIVE MEASURES ux Y : b«CAT : ( »1) »TP«u: i510
VAW1A6LE N MINIMUM MAXIMUM «£AN sTD OEV
9.ALDY 3 l.aOOO S.aoOO J.7667 4.0008
10.MPG 3 -y.sOOU 10.100 ^.9333 .2886tt
11.HC J .1VOOU -1 .
-------
5-26
U.NOX 3 .2*500 .33100 ..10933 .1*038 -1
l&.METHANOL 2 .70000 -2 .13000 -1 .10000 -1 .42426 -2
DESCRIPTIVE MEASURES oxY:o»CAT:(»2>'TPRO:SS10
VARIABLE N MINIMUM MAXIMUM M£AN STO DEV
9.ALDY
10. *PCj
11.HC
12.CO
14.NOX
lei.METHANOL
2 .20000 2.0000 1.1000 1.2729
i. 10.200 10.500 10.3SO .2121J
2 .20000 -1 .21000 -1 .20300 -1 .70711 -3
2 0. 0. u.
2 .1*600 .26700 .23150 .50205 -1
1 .lolOu
.16100
.16100
DESCRIPTIVE "E4SURES <^6> uxr :«»»CAT: (»2) »TPRO:5Sin
VARIABLE N MINIMUM MAAlMUM MEJN STD UEV
9.ALOY
11. MC
12. CO
U.NOX
16«H£THANOL
DESCRIPTIVE *£ASUKES UAY:O*CAT: (»3)
N MINIMUM MAXIMUM
1 l.oOOO l.bOOO 1.3000
1 10.000 10.000 10.000
1 .23000 -1 .23000 -1 .23000 -1
1 .laooo -i .10000 -i .idooo -1
1 .30^00 .304.00 .30^00
1 .22000 -1 .42000 -1 .22000 -1
STO OEV.
9.AUOY
10.MPO
1 l.HC
12.CO
14..MOX
16.METHANOL
OESCHIPTIVE
2 *.oOOO 10.200 10.000 .28284
i. .22000 -1 .*0000 -1 .31000 -1 .1272S -1
i. . 1S«»00 .23500 .19450 .37^76 -1
2 .4iOOo -1 .*5000 -1 .43000 -1 .23234 -2
oxY:j«CAT:(*3>»TP«o:SSI0
N MINIMUM MAXIMUM MtAN STO UtV
-------
5-27
9.ALDY
10.MPG
11. HC
12. CO
U.NUX
16.METMANOL
DESCRIPTIVE MfcASUKES
VAPIA8LE
9.ALOY
1 0 . MPG
11. HC
12. CO
14.NOX
16.METKANOL
1
3
3
3
3
1
<<
N
2
1
2
2
1
0
64.400
V.6000
•2900U
0.
.2790U
.36000
#9> OXY:
MINIMUM
293.06
*.dOOO
.1U200
.10000
.2beOO
64.300
9.SOOO
-1 .^0000 -1
.22200
.33WOO
•1 .36000 -1
5»CAT: i«3) »TP»C
MAXIMUM
294.49
9.dOOO
1.0000
•2 1.0000
.25AOO
64.800
9.7000
.blOOO -1
.74333 -1
.30067
.36000 -1
):SSlu
MEAN
293.77
9.8000
.55100
.50050
.-25800
.10000
.34395 -1
.12788
.JoOOo -1
STU OEV
1.0112
.63498
.70640
DESCRIPTIVE MEASUK6.S <100> OXY:O«CAT: («4) »Tpno:SS10
VAWIA8UE N MINIMUM MAXIMUM MEAN
3 fi.1300 41.530
3 9.7UOU 9.aOOO
3 .33000 -1 .17600
STD OEV
3
20.337
V.7667
.10400
<2.a90?
9.ALDY
10.MPG
11.HC
12.CO
U.NOX
Ib.METrtANOL
DESCRIPTIVE MEASUHtS <10l> UXY :3»CAT : («4) «TP-<0:SS10
VARIABLE N MINIMUM MAXIMUM MtJN
9.ALOY 2 -1
.71505 -I
1.0B10
3 .SUOOO -2 .41000 -1 .25333 -1 .184<»a -1
1 .Hl'700 .51700 .51700
5TLi OEV
11.031
.35355
2 .20000 -i .J6000 -1 .1^000 -1 ,
-------
5-28
16.METHANOL 0
INSCRIPTIVE MEASURES <102> OXY :5»CAT: <»4) «TPHO: SS10
VAPIA8LE N MINIMUM MAXIMUM M£AN STO OEV
V.ALDY
IO.MPG
ll.rtC
12.CU
1«..NOX
16.METMANOL
DESCRIPTIVE MEASURES
VARIABLE
9.ALDY
IO.MPG
ll.rtC
12. CO
14.NOX
16.METMANOL
DESCRIPTIVE MEASURES
VARIABLE
9.ALDY
lO.MPf,
ll.rtC
12. CO
14..NOX
16.METHANQL
2
2
2
*
• 2
0
<
N
2
1
2
2
2
0
<
N
0
1
2
2
*
0
01.200
9.6000
.30000
.30000
.2370U
10j> OXY:
MINIMUM
69.300
10.300
.26100
4.*16U
.20600
lo«»> OXY:
MINIMUM
10.100
.2*70U
3.J190
.2060U
134.30
9.7000
-1 .61000
-2 .21000
.2000U
O*CAT: i»5>
MAXIMUM
82.050
10.300
.30300
5.3980
.2^600
3»CAT: (»5)
MAXIMUM
10.100
. J7&00
3.23oO
.J2300
107. as
V.6500
-1 .4*1500 -1
-1 .12000 -1
.24850
•TM,0:SS10
MEAN
75.675
10.300
.28200
3.1570
.29100
«TP*0:SS10
MEAN
10.100
.33150
5.1520
.30450
37.689
.70711
.17678
.12728
.16263
STU OEV
V.0156
.29098
.J*oa3
.707U
STU OEV
.02VJ3
.Id950
.2616J
-1
-1
-1
-1
-1
-2
-1
-1
DESCRIPTIVE "EASUWES <10a> OxY:S»CAT: («5)«TP«0JSSI 0
VAHIABLt N MINIMUM MAXIMUM MEAN STD OEV
9.ALDY 0
-------
5-29
10.MPG
ll.fiC
12. CO
14.NOX
U.METHANOL
DESCRIPTIVE MEASURES
VAWIA8LE
9.ALDY
lO.MPf,
11. MC
12. CO
14.NOX
liS.MfcTMANUL
OESCHIPTIVE MEASURES
VAPIA81?
9.ALHY
10.MPG
11. MC
12. CO
14.NOX
16.METHANOL
DESCRIPTIVE M&ASUKES
VAPU8LE
9.ALOY
10.MPC,
ll.MC
12. CO
14.NOX
16.METHANOL
2 V.VOOO
2 .53100
2 a.-*050
2 .34*00
u
•<100> OXY
N MINIMUM
U
2 10.10U
2 .64300
2 '.8250
2 .30500
0
<107> OXY
N MINIMUM
0
2 10.00U
2 .54JOO
4 7.8760
2 .29300
0
<10a> UXY
N MINIMUM
0
2 9.VUOO
2 * 60bO 0
2 a . y ti^*0
2 .307uu
0
10.10U 10.000
.6490U . 5<*OUO
9.753U ^.0790
.34100 .33500
:O»CAT: <»6)*TPKO:SS10
MAXIMUM Mt'AN
10.10U 10.100
.6710U .64950
7.V8VO 7.a070
.J080U .30650
:3*£AT: («6> »TPHO:SS10
MAXIMUM MEAN
1U.100 10.050
.57500 .55900
3.652U 0.1640
.30100 .29700
:^CAT:,.6)M,,o:SSlu
MAXIMUM M£4N
10.100 10.000
.67700 .64250
a.^OdU a.i460
.3220U .314SO
.14142
.12728 -1
.V5JKJ
.B4fl53 -2
STO OEV
.30406 -1
.45739
.21413 -2
STD OEV
.70711 -1
.22627 -1
.69014
•365o9 -2
5TD i>EV
.14142
.46790 -1
.07,81 -1
.10607 -1
-------
5-30
DESCRIPTIVE MtASuKES <10"»> OXY : 0»CAT:(*7)«TPnO:SSI 0
N MINIMUM MAXIMUM
STu OEV
9-.ALOY
10.MPG
U.rlC
12. CO
U.NOx
Ift.METHANOL
DESCRIPTIVE -EASU
VAPIA8LE
9.ALDY
1 0 . MPfj
11. HC'
12. CO
l^.NOX
lo.METH.NOL
DESCRIPTIVE MEASU
VARIABLE
9.ALOY
1 0 . MP<3
---ll.rlC
12. CO
U.NOX
1S.-6TH.NOL
DESCRIPTIVE MEASU
VWIA8LE
^.ALDr
10.MPG
11.. -!C
0
J
3
3
3
0
WES <1
N
0
2
2
<
2
0
'WES <1
N
1
2
3
j
2
r.
v
HltS <1
N
U
2
2
10.100
.3*000
£.0140
.10000
10> OXY:
M I N I MUM
10.000
.71000
.21000
.27900
11> OXY:
MINIMUM
10. 100
*.-»000
. 10600
. 1UOOO
.^10U
12> UXY:
M I N 1 MtJM
*.VOOO
.1^700
10.100
-1 .2&500
2.^2*0
-I .".6000 -1
3»CAT: <«7) »TPh(0
MAXIMUM
10.100
-1 . 7*000 -I
-1 .35000 -1
.29100
5»CA|: (»/) »TPKO
MAXIMUM
10.100
10.100
.11200
-I .oenoo -1
. 2 '/ ft u u
O'CAT : (»a) «TPnO
MAAI.MUH
lu.20o
.^VOOO
10.100
.16800
2.2137
.33667 -1
:SS10
M£AN
10.050
.72500 -1
.2POOO -I
.23000
:SS10
MEAN
10.100
10.000
.10900
, i»aOOO • 1
. 27UU U
JSS10
"It AN
10.050
.2«»330
.11635
.20756
.20302 -1
STU OEV
.70711 -1
.21213 -2
.V«C*Vs -2
.1<*1<»2 -2
STO OEV
.!*!*£
.JOOOO -2
.
-------
5-31
12. CO
14.NOX
16. METMANOL
iSCHIPTIVE MtASUMtS
VAPlAbLE
9.ALOY
10. MPG
11. MC
12. CO
14. NOX
16. METMANOL
SCHIPTIVE MEASUKES
VARIABLE
9. ALDY
10. MPG
il.MC
12. CO
U. NOX
16. METMANOL
2
2
0
6.* OXY:
N
0
2
2
2
2
0
<
N
5
*
s
5
s
1
MINIMUM
*.BOOo
.21600
*.26lO
.29100
11S> OXY:
MINIMUM
106.65
9.VOOO
.3*600
.40800
•2olUU
1.0400
6.tt3VU
.^800
3»CAT: (*8)*TPKO
MAXIMUM
10. luu
.5*800
9.6010
.3670U
0»CAT :NONt»TPHO
MAXIMUM
2*6.62
10.200
.60200
9.7060
.30500
1.0*00
6.6650
.29300
:SS10
MEAN
*.9iOO
.38200
9.*310
.30*00
:SS10
MEAN
1*4.65
10.000
.^7720
J.07SO
.31820
1.0*60
.24607
.*24*6 -2
STO OEV
.^1213
.23476
.24042
.tt202* -I
STO OEV
4 OXY :Q»CAT : ( «U «TP«0: SS20
VAWJA8LE N MINIMUM MAXIMUM MEAN STO OEV
9.ALDY 2 .70000 2.tfOOU i.*500 1.0607
lO.MMr, 2 19.000 H.300 19.700 .1*1*2
11.HC e. .50UOO -2 .liOOU -1 .80000 -2 .*2*26 -2
12.CO 2 .rtOOOO -2 .2bOUO -1 .16500 -1 .12021 -1
U.NOX 2 .flOOOO -2 .iJOOO -1 .30500 -1 .J1820 -1
16.METMANOL 2 .loOOO -1 .2200U -1 .1*000 -1 .*2*26 -«»
DESCRIPTIVE M
<122> OXY : 3«CMT: ( «1 ) »TPKO:SS20
-------
5-32
VARIABLE
Y.ALDY
10. MPG
ll.rtC
12. CO
14. NOX
16. METHANOL
DESCRIPTIVE MEASUKtS
VARIABLE
9.ALDY
10. MPG
11. HC
12. CO
14. NOX
16. METHANOL
DESCRIPTIVE MEASUHES
VARIABLE
9. ALDY
10. MPG
ll.rtC
12. CO
14. NOX
16.METMANOL
N
2
3
3
3
3
3
<
N
2
I
2
2
2
1
<
N
2
2
2
2
2
1
MINIMUM
l.OOOU
19.400
. 10000
U.
.41300
.40000
1 UXT
MINIMUM
1.1000
U.400
.70000
0.
.4^00
.20000
124> UXY
MINIMUM
.00000
19.AOO
.*0000
U.
.1 3300
.3VOOO
MAXIMUM
2.000J
19.300
-1 .JVOOO
.27900
.b-4000
-2 .J6000
:S«CAT: ui>
MAXIMUM
1.6000
1 V.40U
•2 .dOOOO
0.
.^200
-2 .20000
!0»CAT: (mi.}
MAXIMUM
1.5000
20.300
-2 .10000
0.
.41300
-1 .39000
MEAN
i.aooo
19.567
-1 .20000 -1
.9333J -1
.47767
-1 .15000 -1
.T,Ko:sS20
M£AN
1.3SOO
19.400
-2 .75000 -2
u.
.47000
-2 .20000 -2
•TPKO:SS20
MEAN
1.1500
19.9&0
-1 .90000 -2
0.
.2/300
-1 .39000 -1
STL) OEV
1.1314
.<0817
.16462
,1607V
.63532
.1&193
STu UEv
.JS355,
.70711
.31113
STO OEV
.49*97
,<»9497
.1414^
.19799
-I
-1
-1
-3
-1
-2
DESCRIPTIVE MEASURE? <126> OXY!5<
VAMA8LE N MINIMUM
9.ALDY i i.iooo
10. MPG i i-y.40o
ii.MC i .10000 •-;
12.CO 1 .90000 -<
MAXIMUM
l.bOOO 1.5000
1^.400 l-y.-OO
.lOOOu -1 .luDOO -1
.VOOOO -
-------
5-33
14.NOX
16.METH4NOL
1 .47100
1 .10100
.47100
.10100
.47100
.10100
DESCRIPTIVE MEASURES <127> OXY:O»CAT: <»3>«TVHO:SS20
N MINIMUM MAXIMUM M£AN STO OEV
0
2 If..900 19.000 18.950 .70711 -1
2 .11000 -1 .30000 -I .,20300 -1 .13«»J3 -1
2 .46100 .601*00 .52750 .10819
2 .51000 -1 .56000 -1 .53500 -1 .j535b -2
9.ALOY
10.MPG
11.HC
12.CO
14.NOX
16.METHANOL
DESCRIPTIVE "EASUKES <12u> OXY : 3»CAT: ( »J)
VAWIA8LE N MINIMUM MAXIMUM
9.ALOY
10.MPG
11. nC
12. CO
U.NOX
16.METHANOL
S7U 06.V
M£AN
1 70.S8U 7Q.5dO 70.5MO
3 lM.400 IV. 200 13.800 ."0000
3 .12000 -1 .29000 -1 .19667 -1 .O&217 -(>
3 0. 0. U.
3 .^JOOO .53800 .4*1167 .54151 -I
'<£. .47000 -I .55000 -1 .51000 -1 .56369 -2
STD OEV
DESCRIPTIVE «£ASU«£S <12*> OXY:5«CAT:(*j)•TPHO:SS20
VAHIA8LE N MINIMUM MAXIMUM M£AN
9.ALOY
lo. MPr,
11.DC
12.CO
14.NOX
l^.MtTHANOL
i. 144.94 103.52
2 17.700 1-f.lOO
'e. .97000 -I ,17<»00
2 .90000 -2 .30900
2 .36000 .42300
155.23
.13550
.15900
.4Q150
.^1213
.J0406 -1
VARIABLE
Oxr:
N MINIMUM
MAXIMUM
STU OhV
-------
5-34
20.800
Is. 100
.13400
OXY:3»CAT:
VAPIA8LE N MINIMUM MAXIMUM MEAN STL) OEV
2 *1.500 113.60 102.55 15.027
2 10.500 ltt.900 18.700 .28284
-1 .55000 -1 .*7000 -1 .11J14 -1
9.ALDY
10.MPG
11.MC
12.CO
U.NOX
Ib.METHANOL 0
DESCRIPTIVE MEASUHES <132> OXYt5»CAT:
VARIABLE N MINIMUM MAXIMUM
9.AUOY
10.MPG
11.MC
12.CO
U.NOX
16.METHANOL
2 .90000 -2 .18000 -1 .13500 -1 .o3o*0 -2
2 .30^0o .43900 .42400
MEAN
1 13d.90 138.90 138.90
1 iS.OOO Id.600 U.600
1 .39000 -1 .3*000 -1 .39000 -1
1 .laOOO -1 .laOOO -1 .IHQOO -1
1 .37<»00 .37<»0y .37^00
0
STD OEV
DESCRIPTIVE M£ASUKES <13J> OXY:o»CAT:!«5)«TPHO:SS20
VARIABLE N MINIMUM MAXIMUM M£AN
STO OEV
9.ALDY
1 0 . MPQ
ll.rtC
12. CO
U.NOX
1
1
1
1
1
61.380
19.500
. <2*500
3.J950
.43200
61.380
IT. 500
.29500
3.0950
.^5200
01.330
19.500
.29500
J.OS50
.4b200
-------
5-35
16.METHANOL
u
DESCRIPTIVE MgASUHtS <13<»> OXY:3»CAT:(•5>«TPKO:SS20
VARIABLE N MINIMUM MAAlMUM MEAN
9.ALOY 0
DESCRIPTIVE "EASUHES <^7> OXY:3«CAT: ( ««j) »TPHO: SS2U
VAWIASLE N MINIMUM MAXIMUM
9.ALQY 0
STD DEV
10.MPG
11. nC
12. CO
U.NOx
IO.METHANOL
DESCRIPTIVE MEASURES
VAPIAdLE
9.ALOV
10.MMC,
H.MC
12. CO
U.NOX
16.METMANOL
DESCRIPTIVE MEASURES
VAOU8UE
9.ALOY
1 0 . MPr,
ll.rtC
12. CO
U..NOX
16.METMANOL
1 18.VOU la. 900 16.900
1 .4 OXY:O»CAT: (*o)»TP*0:S520
N MINIMUM MAAlMUM HgAN STO OEV
0 ....--
2 18.700 19.300 19.000 .42426
2 .5-500 .b-rftOu .57050 .J6062 -1
2 <+.l*7u 4. 22*0 -.2115 .20b06 -1
2 .50700 .31500 .51100 .3656S> -2
0
STu OEV
-------
5-36
10
11
12
14
16
.MPG
.HC
.CO
.NOX
.M£THANOL
DESCRIPTIVE MEASURES
*
10
11
12
14
U
VARIABLE
.AUOY
.MPG
.HC
.CO
.NOX
.METHANOL
DESCRIPTIVE wEASUHES
9
10
11
12
14
VAHIABLE
.ALOY
.MPG
.HC
.CO
.NOX
2 18.800
2 .50000
2 J.6650
2 .t/tfOU
0
<13o> OXY
N MINIMUM
0
2 IV. 100
2 .44400
2 J.0620
2 .42000
0
<139> OXY
N MINIMUM
0
3 U.900
3 .32000
3 .4^00
3 .2JOOO
IV. 100
.b4200
4.4530
.5bOOU
:5»CAT: <**)
MAA.IMUM
IV. 400
.47000
3.3080
.40800
:O«CAT: <«n
MAXIMUM
IV. 400
•1 .10800
1.2110
-I .12400
i8.950
.'52100
4.0MO
.51400
•TPM:SS20
«fcAN
19.250
.4b700
3.7350
.45400
*TPHO:SS20
MEAN
19.100
.87333 -1
.85400
.-.7333 -1
.21213
.2969B
.55720
.bOV12
aTD OEV
.21213
.10385
.10324
.48083
STO u£V
.26458
.71452
.39729
.3774*
-1
-1
-1
-1
-1
-1
!6.MtTHANOL
DESCRIPTIVE *EASUKES
VARIABLE
^.ALOY
10.MPG
11.HC
12.CO
lu.NOX
16.METHANOL
:140> OXY:3»CAT: (
MAX I
»TPHO:S520
5TJ OEV
2 18.900 IV.400 19.150 .J5355
2 .74QOO -1 .11300 .96000 -1 .31113 -1
2 .loOOO -1 .ioOOu -1 .38000 -1 .^8284 -I
2 .34000 .38400 .36600 .^'s+'sti -1
-------
5-37
DESCRIPTIVE
VARIABLE
9.ALOY
10.MP6
11.MC
12. CO
14.NOX
liS.METhANOL
OESCHIPTIVE
VARIABLE
9.ALOY
OXY;S»CAT:<»7>»TPKO:SS20
N MINIMUM MAXIMUM MEAN STD OEV
0
3 19.000 IV.600 19.300 .30000
3 .36000 -1 .12800 .8bOOO -1 .46293 -1
3 .10000 -2 .90000 -2 .60000 -2 .OseV -2
3 .36800 .44J>00 .40667 .J7112 -1
OXY:O«CAT: (»e)
MINIMUM MAXIMUM
STD OEV
lO.MPQ
11. MC
12. CO
U.NOX
16.METMANOL
OESCWiPTIVE MEASURES
VARIABLE
9.ALOY
10.MPG
11. HC
12. CO
U.NOX
1&.ME7HANOL
OESCHIPTIVE MEASUHES
VARIABLE
9.ALDY
1 0 . MPG
11. HC
2
2
2
2
0
18.400
.2obOO
J.40IO
.42600
<143> OXY:
N
0
2
2
2
2
0
< J
N
8
7
d
MINIMUM
10.800
.1VSOO
>..1^0
.31700
L45> OXY:
M I N I MUM
7.3.740
19.100
.34JOu
19.500
.J2300
3.4240
.*2600
3«CAT: (•«) »TRHO
MAXIMUM
1.V.400
. J090U
4.31VO
.3J40U
0*CAT:NONt»TP«0
MAXIMUM
165. «
21.100
.47700
18.930
.30400
3.412S
.42eOO
JSS20
MEAN
IV. 100
.2S3SJO
4.2590
.32530
:SS20
MEAN
126. vft
IV. 357
.39612
.77782
.26670
.16263
STD OEV
.42426
.734^
.B4853
.12021
STD OEV
J*.2bl
.69727
.J8200
-1
-1
-1
-1
-1
-1
-------
5-38
1?.CO
lO.NOX
l6.M£TrlANOL
otscHipTivE MEASURES
VARIABLE
9. ALPY
10. MHO
11 ."C
12. CO
10. NOX
16.M£THANOL
OESCHlHTIVt '1EASUKES
VAklA&LE
9. ALOY
1 o . MPC,
11. MC
12. CO
lO.NOX
l&.MfcTHANOL
OE5CHIPTIVE -EASUHES
VAWU&LE
4. ALOY
10 .MQfi
ll.nC
12. CO
lO.NOX
lh.M£TH4NOt
a <».*no 6.05*0
3 .07500 .57900
, .«.00 1..1VU
OXY : 3*CAt:i<40Nt»TPHO
N MINIMUM MAXIMUM
3 a^.aoo l3l.2o
3 19. .00 1^.900
3 .33^00 .3*900
3 3.0130 <».3l2o .
3 .^200 ...-600
3 .01600 1.29rtU
<1^7> OXf :S*CAT'.NONt»fHKO
N MINIMUM MAXIMUM
2 10H.20 103. *0
2 1^.900 l^.lOo
d «3^dOO .3*»*»oo
j; <*.jo70 (*.(*230
2 .*» L'XY: O»CAT :STOCX»THK
N MINIMUM MAXIMUM
o .20000 .30000
o ir-vOC l^.Suo
<» .50000 -2 .10000 -1
<» .13000 -1 .i5000
«» 0. .30000 -2
<* .10000 -2 .50000 -2
0.7681
.30537
..CO 75
:SS20
M&AN
122.27
19.633
.33e&7
..05V3
.07033
1.0033
= SS20
MEAN
105.05
19.000
.33500
..3660
.03200
1.1910
u:SS20
ME»N
.^2500
i9.37b'
.70000 -2
.^7SO -1
.12300 -2
.c;7500 -7?
.73652
.36300 -1
.1677sJ
sfU OEV
jo. 030
.25166
.80829 -2
.<0956
.^7099 -I
.23776
sTO OEV
1.2021
.1010^
.12^B -I
.0J039 -1
.70711 -2
.13132
STO OEV
.30000 -1
.36030
.*•<•<* -d
»o6d3b -I
.£3000 -2
.i^07a -2
QtSCHIPTlvt
OXY:U«CAT:
-------
5-39
VAPIA8LE N
<».ALDY 2
IO.MPG 2
11.. -1C 2
12. CO 2
U.NOX 2
16.METHANOL 2
OESC«IPTIV£ MCASUKtS' <
VA-lAdLE N
9.ALOY 3
lO.MPf, 3
11. MC 3
12. CO 3
l<».NOx 3
Ifc.METHANOL 3
DESCRIPTIVE MEASURE*; <
vAcuate N
9.ALOY 2
in.MPr, 2
11 .MC 4
12. CO 2
1<».NOX 2
l6.MiTH.NOL 1
JESOMPTIve -ASUKCS <
VARIABLE N
a.ALDY 2
1G.MP-- 2
11.- iC 2
12. CO 2
rtlNlMU*
.3UOOO
21.500
.20000
.1 7000
.20000
.20000
l34> UXY
MINIMUM
. -yOuOO
21 .20u
.HOoOU
0.
l.i<»0u
.20000
15J> UXY
MiNlMlW
.60000
41.200
.etuOOO
u .
1.174U
. JuOOO
13'»> OAT
MINIMUM
.50000
41.000
.ooOOO
u .
MAXIMUM
."0000
21.600
-2 .JOOOO -2
-1 .4bOOO -1
-2 .50000 -2
-2 .aOOOO -2
:3»CAT: («i)»Tr'«
MA A I MUM
3.000o
21.600
-2 .^0000 -2
.10000 -2
r.ciso
-2 .auOOO -2
:5*CAT: («1 ) «TP»?
MAXIMUM
2.£00u
21.<.00
-2 .oOOOO -Z
0.
1.4620
-2 .JOOOO -2
: O'CAT : ( »2) "Ti^
M»Al«UM
a.7000
21 .70o
-2 .70000 -4
.^JOOO -1
MEAN
.33000
41.550
.25000
.22300
.3SOOO
.30000
u: SS30
MtAN
2.2000
41.03
.«JJ33J
.33333
1. 1B«J
.3ett&7
0:SSJO
MtAN
l.^OOO
41.300
.aooou
0.
i.aibo
.30000
0 : iS30
^EiN
J.6000
^i.J30
.65000
. I Is'OO
STU Utv
.70711
.70711
-2 .70711
-1 */77b2
-2 .4121J
•2 .'»2'»2&
STU OEV
1. U58
.20617
-2 .377JS
-3 .3773s
.*19ji
-2 .15275
STU OtV
1.1 Jl*
.1<*1<.2
-2
.04225
-2
STu UEv
«».3a*»i
.^-97
-2 .70711
-I .Ib2o3
-1
-1
-3
-2
-2
-2
-3
-3
-1
-2
-I
-3
-1
-------
5-40
VAOIABLE
11.HC
12.CO
14.NO*
16.METWANOL
H .3*500 .36200 .-7350 .lldO*
1 .2«»OOU -1 . OXY!5«CAT:(*4) «TMWO:SS30
ft MINIMUM MAXIMUM M£AN STO OEV
1 b.oOOU 5.6000 b.OUOU
1 20.300 2U.300 CO.300
1 .luOOO -1 .1000U -1 .lUOOO -1
1 .2*000 -1 ,OOJ .219SO .<»313<' -1
2 .27000 -I .6XOOU -1 ,<.^000 -1 .2<*0<*ii -1
u
STO 0£V
1633
OXY:3«CAT:(»j)«
N MINIMUM MAAlXUM
1 70 . 7u
-------
5-41
9.4LOY
10.MUG
11.HC
12.CO
14.NQX
Ib.METHANOL
O.ALDY
1 0 . MPfi
H.HC
12. CO
Ih.METMANOL
VACIA3LE
10.MPG
11. HC
12. CO
U.NOx
16.HJ.TH6NOL
VAPI ABLl
9.ALDY
1 0 . MHr,
11.HC
12.CO
2 Vft.950 ll^.^e
2 U.bOO 20.800
£ .24000 -I .10001-
2 .ouOOO -2 .12300
2 J..O&40 1.2240
0
OXY:U«CAT:(»4>«
N MiNiMUM MAXIMUM
2 j.£ooo 3.780o
2 £0.£UU 20.400
11.JJ5
.62000 -1 .33740 -1
.o^SOO -I .82731 -1
i.lbeO .*61a7 -1
M£ AN
J.5300
£0.300
STD U£V
.J53S3
.14142
2 .UOOU -1 .14000 -1 .13500 -1 .70711 -J
2 .4/500 .02700 .55100 .10?4tt
£ .5000U -2 .lOOOu -1 .7^000 -2 .JS355 -2
1 .3oOOO -I .JftOOO -1 .36000 -I
OXY:3»CAT:(«4)«TPHU:SS30
IM MiMlMUM MftXlMUM "f. 4N STD 0£V
2 l4.aOu 21.bOO IS.200 4.dOdJ
£ £0.400 20.700 £0.550 .2121J
2 .VOOOO -2 .100UU -1 .-55000 -2 .'/0711 -3
2 .60000 -2 .oOOOO -2 .60000 -2
i.0'34b .'•030b -1
0
< lb£> OXY : 3«CAT : ( »«*) ••
^ MINIMUM *»AAlMljM
1 £2.^00 22.50U
1 £'.).7QO 20.700 £0./00
1 .11000-1 .liuuu -1 .11000-1
1 .7uuOO -2 .7UOOU -2 .7UOOO -£
1 1.J7JO 1.0730
-------
5-42
16.METHi.NOL
MEASURES OAY :o»C«T : ( «;j) «TB*u:iS30
VAPIA&LE N MINIMUM MttAlMUM MEAN STU JEV
9.Al_L'Y
IO.MPG
ll.rtC
12. CO
U..MQX
Ife.METHANOL
1
1
1
1
1
0
Jb.ObU Jo. 050
(Sl.sOO 21.500
.6OOOO -1 .btoOOu -1
2.1490 2.19*0
1 . 104U 1 . 10VO
JB.050
tfl.aOO
.06000
c.1^0
UlOwu
-1
OtSCHIPTlVE
10.MPG
11. MC
12. CO
IS.MtThANOL
:3»CAT : ( ••$) <
N MINIMUM MAAlMUM
0
1 il. OXY:?
N M I N I MUM
0
O*Y : o«CAT : < »*) «TPnu:SS30
N MINIMUM MAXIMUM «tiM STO J£V
o
-------
5-43
10.MPO
11. HC
12. CO
1<..NOX
16.METHANOL
DESCRIPTIVE MgASUHES
VAPJA3LE
9.ALOY
10 .MPG
11. HC
12. CO
l OXY:3«CAT: ( »6> »TP«o: SS3o
Mi N I MUM MAAlMIJM w£4N
20.bOu 21.000 iO.vOO
.40*00 .41200 .ulOOO
H.J420 5.0560 -*.6990
1.107U 1.1190 1.11JO
16«> OXY:S»CAT: (»6) *TPKO: SS30
MINIMUM MAXIMUM ME*N
iO.500 21.300 <:0.900
.2eeOw .379UO .33150
3.<»56u 4.3700 J.9130
.aloou 1.1130 .96450
le^> OXY s o*CAT : ( a7) «TPH(j: SS30
MINIMUM MAXIMUM -EAN
2Q.70U 20.900 iO.rfOO
.9UOOO -2 .1BOOO -1 .13000 -1
.40200 l.J3^0 1.12AO
.luOOu -1 .JOOuo -1 .13333 -1
.2121J
.OJ04u -2
«tf467b
«4^<«2d -2
5Tu UEv
.1414^
.^284 -2
.304^
.a4rtSJ -2
STU OEV
.36569
.olald -1
.0*0 JO
.^1001
iTu -2EV
. 10000
.»»5a26 -2
.^4031
.:o*o« -i
-------
5-44
OESCHIPTlvE
OXY:3»CAT:<«7>
N MINIMUM MftAlMUM Mt'AN bTU
0
2 il.uOu 21.40u OXY:5*CAT:(*7)
VARIABLE N MIMMUM MAXIMUM
9.ALOY
lO.MPf,
H.HC
12.CO
14.NOX
14.METHANOL
0
3 21.000 21 .<»00 £1.167
3 .90000 -2 .VOOOO -2 .90000 -e
3 0. .11000 -1 oe>6ft7 -;
3 1.0130 1.1110 1.0677
0
STD OtV
.20817
.^5076 -2
-1
DESCRIPTIVE MfASUHES
VAPIA8LE
9.ALOY
1 0. I*MG
11.HC
12.CO
0 X Y 11
N MINIMUM
2 tfO.VOO
i .^7100
MAXIMUM
21.900
.2J300
<».0900
l.K
MEAN iTU OEV
.70711
.22700
-2
-2
-1
16.*tTHANCL
MINIMUM
0
2 il.-*00
2 .U100
MAXIMUM
S^.OOU
«£.AN 3 I'D OEV
il.vSO .70711 -1
.i
-------
5-45
12. CO
14.. NOX
16.METHANOL
DESCRIPTIVE **ASUHE.S
VAPIAHLE
9. ALOY
10.Mfr> OXY:
N MINIMUM
o 72.^60
7 19.800
8 .3JOOU
d 4 .£o5u
a 1.U88U
4 . 7 ?30u
< l ^o> OXY :
N MINIMUM
3 10-.OU
3 20.bOU
3 .31-00
^ "».i22v
j 1 . i<* 70
J .N^OU
<177> OXY:
N MINIMUM
3 1 0 / . 1 u
3 ».200 J
1.2420 1.1963
,^<»0u .H6967
,.CAT:NONt.>rP,u:sS30
MAXIMUM »E4N
IJu.bO ilb.JU
21.2JU cl.133
. 3230o . 32 1 OU
4.bi9u +.3&'iQ
l.illU 1.1MO
.VJOuu .91267
.36416
.-»! H9 -1
•jTU DfcV
J4.a3u
. 3^442
. £. 7396 •!
.39097
.74517 -I
.01429 -1
STO OEV
21.770
.o2*bO
.U06y -1
.08189 -1
.-7606 -1
.38527 -l
STU OEV
lJ.262
.113-7
.iOOOO -2
.lbb/3
.
-------
5-46
*
10
11
12
14
16
VAWIABLE
.ALOY
.MHG
.HC
.CO
.NOX
.METHANOL
OtSCKIPTIVE MEASUHES
9
10
11
12
U
U
9
10
11
12
14
!*
VARIABLE
.ALDY
.UPC.
.HC
.CO
.NOX
.METHANOL
*IPTIV£ vEASUKts
VAPIASLt
.ALOY
.MPG
.*c
.CO
..NOX
.MEfMANOL
N MINIMUM MAAlMUM
4 .4UQOO i.aOOU
4 20.VOO 21.700
4 .4UOOO -d .oOOOO -2
4 .=,7000 -1 .6S>000 -1
4 U. .70000 -2
4 .UuOO -2 .90000 -2
< OXY:O»CAT:,NONC.«TPK
N MINIMUM MAA!MUM
2 160.30 1/0. bO
2 19.300 21.600
2 .30<»00 ,3290u
2 3.4130 4.07t>0
2 1.5330 1.0980
2 .7c200 .-*260G
<20o> OXY : 3»C*T :\ONt«TP«
N MINIMUM MAAlMUM
2 m.*o 150. vu
3 Isi.aOO 20.600
3 .24^00 .19900
3 J.ao5u 4,£<»50
3 1.6010 1.093U
3 .77,00 .V.700
MEAN
1.7500
il.JSO
.32500
.61bOO
.22500
.55000
0:SS40
MEAN
166.40
iO.550
.31900
3.9445
1.6405
•624UO
0 ! SS40
M£.N
135.40
£0.167
.29267
4.0640
1.6443
.a,9,7
STO OEV
1.07SB
.41231
•2 .V574J -3
-1 .34467 -2
-2 .33040 -2
-2 .41231 -2
STD u£v
2.969U
1.4d49
.14142 -1
,1SD»7
.81317 -1
.14425
sro JEV
21.920
.40415
,bS076 -2
. 1V064
.^6231 -1
.56312 -1
OESC-IPTIVE «£ASU*ES «07> 0*r : g.C-T SNONi-TP^o : SS^O
9
10
11
12
VAPIA8LS
.ALDY
. MPr,
.rtC
.CO
N MINIMUM MAAlMUM
3 113.30 11V.6U
3 19.400 20.200
3 .2^300 .30700
3 3.d95u 4.074U
-£AN
116.83
iv.a67
.2^367
J.V7V3
5TU OEV
3.0892
.41633
.12220 -1
.av94S -i
-------
5-47
U.NOX
16.MS.THANOL
VARIABLE
Q.ALOY
lO.MPr,
ll.nc
12. CO
3 1.&270
3
1.7610
.&7002 -1
16.METHANOU
0 .«0767
< OXY:O«CAT:STOCK»T?*U:SS«»O
N MINIMUM MAAlHUM MEAN STU OEV
4 0. .o<»OUO .42000 .28612
•<» .01305
•• .10000 -2 .JOOOO -2 .20000 -2 .alorO -3
to 0. .36000 -1 .20000 -1 .15663 -1
<• .laOOO -1 .2b60o .tt^SOO -1 .11220
<• .10000 -2 .20000 -2 .IsuOO -2 .37735 -3
-------
NUIIhtH
Ufr MlLilliiAN ItHMlNAL SVSFEM IMGOEU AK173)
I3:0bib<. EOT
WEU MAY 11/83
MMMMM
MMMHMMH
MMMMMMl-IMM
MMMMI1 MilMMM
MMMHM MMMHH
MMMMMMMMMMM
MMKKMMMMM
MHMHM.Ii-l
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15.MC.NM 2 .10*20 .1159U .11005
DESCRIPTIVE MEASUKtS <2> Oxr:j«CAT: <»l)»TPno:KrP
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15..1C.NM 3 .10020 .1227U .11277
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15.nC.NM •* . lOJSu .1-lSO .118V2
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15.rlC.NM 1 .1<>**0 .lt**0 .14**0
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VAWlttBLE N MINIMUM MAXIMUM M£AN
15.nC.~JM 3 .11530 .12990 .12380
VAWIA8LE
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1 .U020
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2 .la07u .ISb^O .1=3*5
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1S.HC.NM
1 .1*300
.1V300
.19300
DESCRIPTIVE M£ASUH£S <10> OXY : 0»CAT :<»<•.) »TP«0 : KTP
VARIABLE N MINIMUM MAXIMUM M£AN STD OEV
I5.HC.NM 2 .1<»920 .15770 .15345 .60104 -2
DESCRIPTIVE "EASUHtS
VAHIABL5
15.HC.NM
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VARIABLE
1> UXY : 3»CAT :(»<») »TPHO: r TP
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.U400 . l«»6au .14040 ,*0510 -2
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VARIABLE N MINIMUM MAXIMUM MEAN STO OEV
IS.MC.NM 2 .2fcobU ,27<»40 .27060 .a37<»0 -2
DESCRIPTIVE- M
DESCRIPTIVE
15.nC.NM
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VA=IA8L£
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3 .3S200 .Jo<»00 .359««o
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MINIMUM MAXIMUM «£AN
<: .•i'njau .s'JTuu ,a9510
TP
M£4N
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STu OEV
-2
3TO OEV
STO OEV
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5-52
1S.HC.NM
N MINIMUM
2 .8^560
MAAiMUM
.3*770
MEAN
.86165
DESCRIPTIVE MEASURES UXY : O'CAT : <*7) «TPRG:FTV
VARIABLE N MINIMUM MAXIMUM MEAN
15.HC.NM j .Ib21u .1S>3*»U .17787
DESCRIPTIVE MEASURES <<20> ux Y : 3«CAT : ( «7)
VA&IASLE N MINIMUM MAXIMUM
IS..1C.NM 2 . 1<«03U .1=260
DESCRIPTIVE M£ASU«tS < UXY :b»CAT : ( »7>
VAHIA8LE N MINIMUM MAXIMUM
IS.rtC.^M l .2bllu
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VABIA8L1
15.iC.NM
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N MINIMUM MAXIMUM
2 .*<»SOO .<»71JO
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15.rtC.NM
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VARIABLE
15.rtC.NM
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VAWIA8L-
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«£AN
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.15651 -1
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.d871S -1
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-------
5-53
DESCRIPTIVE M£ASU«ES <27> UXY : b*CA r :NON£«TP3u if TP
VAOlAdLE N MiNiMUM MAXIMUM M£AN STO 0£V
1S.HC.NM a .HJISu 1.116* .97395 . OAY : 0«CAT : 5TOC«»TMKO:FTP
VAPIA8LE N MINIMUM MAXIMUM M£AN STD 0£V
15.HC.NM 2 .UvrtO .1<»6SO .U315 .*727t> -2
0£SC«IPTIVE
VAPlAdLl M MINIMUM M4A1.HUM ^EAN 5Tij L)£V
15.MC.NM 1 .UbOu .i3600 .13eOO
OESCHIPTlvE MEASURES Ol> UXY :o«CAT : (»l )
VAPlA9l.£ N MINIMUM MAXIMUM MEAN STO 0£V
15.rtC.NM 3 .2/000 -2 .3«OOU -2 .31667 -2 .S6862 -3
"E4SIWES <32>
N MINIMUM MAXIMUM M6.AN STO 0£V
1S.HC.NM 3 .5*000 -2 .0*000 -2 .65333 -2 .55076 -3
0£SCVlPTlv£ MgASUKt"? OXY:S«CAT: (»i )
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-2 .aOOUU -2 .67250 -2 .i35S»fl -2
' N MINIMUM MAXIMUM Mfc.AN STU UEV
15.nC.Mw 2 .^ooOy -2 .iiaou -i .d'lOOO -2 .3656V -2
OXY : 3»CAT : ( *2)
VARIABLE N MINIMUM MAXIMUM vt£4N
15.rtC.NM j .72000 -2 .aooou -e .7bOOO -2 .-Jbft9 -3
DESCRIPTIVE M£«5Ur(c.s UAY:b*CAr : («2)
VAPIA8L? N :llNiMUM MAXIMUM M£AN STlj Q£V
-------
5-54
15.HC.NM 1 .33000 -2 .33000 -2 .&3UOO -2
DESCRIPTIVE "EASUHES OXY :0»CAT : <»3>
VARIABLE N .MINIMUM MAXIMUM Mg&N STO OEV
15.HC.NM 2 .S^OOO -2 . /<*000 -2 .6isbOO -2 .19092 -2
DESCRIPTIVE MEASURES UAY:J«CAT: (»3)«TkHO:nwy
VABIA&LE N MlNlMU* MAAl«UM ,M£AN STO OEV
15.riC.NM J .ouOOu -2 . 7100u -t .6b333 -2 .3b076 -3
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15.HC.NM 2 .boOOU -2 .6SOOO -2 .62500 -2 .3b35S -3
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1S.HC.NM • 2 .StfOOu -2 .bbOOO -2 «.3JSOO -2 .21213 -3
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VAPIABLF N MINIMUM MAXIMUM MtAN STU UEV
15.nC.NM 2 .<»700U -2 .72000 -2 .5-ibOO -2 . 1767»' -2
DESCRIPTIVE «£ASUr!f5 <*»2
VARIABLE N MINIMUM MAXIMUM M£AN STU OEV
IS.^C.NM 2 .5'/OOo -2 .03000 -2 .61000 -2 .36569 -3
DESCRIPTIVE W£4SUK£S <«.j> ux Y : o«CA T : ( »5 ) »TPRu : nw Y
VArffASLE N 'MINIMUM MAXIMUM ^tVl 3TU DEV
15.nC.NM 2 .11000 -1 .;<:nou -1 .11=00 -I .70711 -3
VAPIABL? N MINIMUM MAXIMUM ^£aN STO OEV
15.HC.N« i. .^ U/.Y : 3<*CAT : ( »5 )
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5-55
VAPIA8LE N MINIMUM MAXIMUM MEAN ST(j OEV
IS.HC.NM i. .39000 -2 .10000 -1 .^<»50U -2 .77782 -3
DESCRIPTIVE MtaSUHES <«.&> UXY : o»CAT : (»b>
VARIABLE N MINIMUM MAXIMUM MEAN STO 0£V
DESCRIPTIVE MEASURES «•?> OXY : J»CAT : ( »6) »TPnu:n\vY
VAPIABI.E N MINIMUM MAXIMUM MtAN STU 0£V
.1<»«»25 . /2S32 -2
DESCRIPTIVE "EASUKtS <•»«> OAY :5«CAT : ( »6> »TPI UAY:o»r*T :'(»7) •Tf»Ho:nwY
VAPlArtLE N MlMMUM MAXIMUM M£4N STU OEV
IS.HC.NM 3 .60000 -t. .dvOOO -2 .71000 -2 .15716 -2
DESCRIPTIVE "EASUWES oo> UXY : J«CAT: (»7>
VASIA8LE N MINIMUM MAXIMUM M£AN STD OEV
IS.HC.NM 2 .5*000 -2 .b<»000 -2 .53000 -2 .1M<»2 -3
DESCRIPTIVE MtASUHt* <5l> uxY:b«CAT: t»7) »TPP,u:h«Y
VA3IA6L1 N MINIMUM MAXIMUM -l£AN STD OEV
IS.HC.NM 1 .S1000 -2 .slOoo -2 .51000 -eJ
DESCRIPTIVE '-«EASUR£S o2> 'jxr : 0»Ci T : I «b ) «TPKU :nw Y
VAPU8L1 N MiNlMUM MAAl^UM «£iN S TO
IS.HC.NM 3 .13-yOO -1 .
-------
5-56
DESCRIPTIVE M£ASu«tS <*<*> OXY:b»CAT: (»S)»TVkO:rnY
VA»IAbl_E N MINIMUM MAXIMUM M£AN STU OEV
15.HC.NM 2 .lo20u -1 .19300 -1 .17750 -I .21920 -2
OAY :o«CAT :r4UNt*TPHO:n*Y
N MINIMUM MAXIMUM MEAN
l-o .3ol3u
DESCRIPTIVE -i
VAWIA6LE
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VAUIA&Lc N MINIMUM MAXIMUM
15.nC.NM 3 .36100 .J79bu
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MtAN
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DESCRIPTIVE MEASURES OXY :b»CAT :NONE»TPnu:n»(Y
VAaiAaLE N MINIMUM MAXIMUM M£»N STO OEV
IS.HC.NM 2 .3*000 .<.715U .<»307b .37629 -I
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VARIABLE N MINIMUM MAXIMUM M£AN iTD D£V
IS.HC.NM 3 .70000 -3 .12000 -2 .vOOOO -3 .20*56 -3
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VARIABLE N MINIMUM MAXIMUM -<£4N STU OEV
IS.HC.NM i .luOOO -3 .2*000 -2 .15000 -2 .1*79V -2
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: U»CA r : ( »2)
M4Al«UM
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5-57
15.rtC.Ni- 2 . IJUOO -2 .2^000 -2 .laSOO -2 . /77B2 -3
OESCHIPTIvE MEASUKtS OXY : a«CAT :( »2) "T^KO : IDLE
VAPI48LE N MINIMUM MAXIMUM M£4N STU OEV
15.HC.NM 1 .3UOOU -2 .30000 -2 .30000 -2
DESCHIPTIvE MEASUKtS UXY : u«CAT : ( » J) «TPWu : 10LE
VAPU8LE N MINIMUM MAXIMUM MtAN STU 0£V
15.WC.NM 1 .^1000 -2 ,<»IOOU -2 .<*100U -2
0£SC«IPTlv£ "£ASUH£<; UXY: J«CAT : (»3)«T^KU: IDLE
VARIABLE N MINIMUM MAXIMUM ,Vt4N STL) U£V
IS.rlC.NM ^ .SiOOO -2 .7080U -I .31400 -1 .J<»7b<. -1
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VAWIA8LE N MINIMUM MAXIMUM M£AN STO OEV
15.rtC.NM 0
DESCRIPTIVE -tEASURlLS OXY : O'CAT :(»<.) »TPHO: IDLE
VAPUfeLE N MINIMUM MAXIMUM MEAN STO UEV
15.HC..MM <: .17000 -t .1JOOO -1 .7JisOU -2 .79903' -2
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N MINIMUM MAXIMUM MEAN STO OEV
15.rtC.NM £. ,3oOOO -2 .ooOOu -2 .32000 -2 .l'j'799 -2
N MINIMUM -'A A 1 '"U* «C.AN 5Tu 0£v
15.riC.NH 2 .aoijQU -2 .i^^Ou -L .11/30 -1 .-»-»5«»d -
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VAWlAHL?! N MINIMUM MAXIMUM MtAN STU 0£V
15.rtC.NM & . 7^500 -I .ab'cou -I .rt<*ioO -1 .aoofta -2
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VAPIA8LE
IS.HC.NM
DESCRIPTIVE M
VAP1A8LE
15.rtC.NM
N MINIMUM MAXIMUM MfcAN
£ .93200 -1 .i^lyu .11000
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VAVIA8L- "* MINIMUM MAAlMUM Mt 4N
15.-«C.NM i .l
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15.rtC.NM
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.160<»u
MEAN
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VARIABLE N MINIMUM MAAlHUM MEAN STU 06.V
IS.HC.NM J .SUOOO -3 .75000 -1 c.33rt33 -1 .J7863 -1
DESCRIPTIVE "EASUKES UAY : 3»CAT : ( »7) "TP«o: IDLE
VAWIA3LE N MINIMUM MAXIMUM M£AN STU UEV
15.HC.NM 2 .oJUOu -2 .1U9UO -1 .46000 -I ,32s27 -2
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VAW[A8L
15.rtC.NM
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-1 .33500 -I
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1 ..ilVOU -1 .2190U -1 .21VOO -1
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MfcAN 5TO OEV
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5-59
DESCRIPTIVE MEASURES UXY:3«CAT: <»8>»TPPu:iOL£
VABIA8LE N MINIMUM MAXl*UM M£4N STO 0£V
15.rlC.NM 2 .5 uxr:0*CAT:NON£»rP^u:iDL£
VAI>IA&L£ N MINIMUM MAXIMUM MtAN sTu 0£v
IS.rtC.NM 7 .eioOu -1 .ii2^u .930S7 -1 .12V01 -1
DESCRIPTIVE x£ASU^tS JAY: 3»CAT :NUNt"TPko:
VABIA&LE N MINIMUM MAAlMUM MtAN STO OEV
IS.HC.NM I .37100 -1 .B7100 -1 .S7100 -I
DESCRIPTIVE MEASURES UXY :a«CAT :NUN£»TP*O: lOLt
VAklABLE N MINIMUM MAA!MUM M£AN STO OEV
15.MC.NM 0
DESCRIPTIVE MEASUrfES <8tt> OAY:o«CAT:STOCN»ThJWO:iUL£
VAWIA8LE N MINIMUM MAXIMUM MtAN STL) OEV
IS.nC.NM <• .sOOOO -3 1.0000 .2S155 .*»9a97
OESCHIPTIVE "EASUHf; <<»!> UAY : U«CAT : ( • 1 ) «TH«u: 5S10
VAPlAfiLE N MINIMUM MAA!MUM M£AN STO OEV
15.dC.NM 2 .2UOOO -2 . UXY : 3«C4T : ( » 1 ) "IVNUS 3si u
VAPlA8L.^ N MiNiMUN MAXIMUM '-ItAN 5TO D£v
1S..1C.NM J .voUOu -2 .iaOuu -I .13&6? -1 .a32b/ -2
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15.HC.NM i .1UOOO -1 .110UU -1 .10500 -1 .70711 -3
DESCRIPTIVE *£ASUH£S <•*«> UXY tb'CAT : <»2) »THKO: SS10
VAPIAdLE N MINIMUM MAXIMUM MtAN STU OEV
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l .JOUOO -1 .JUOOU -1 .30000 -I
0
N MINIMUM MAAlMUM .vt£AN STU OEV
15.HC.NM 3 .UOOu -1 .75000 -1 .J7000 -1 .J3287 -1
DESCRIPTIVE MfeASUKtS <•»'*> u*Y:s«C4T: (*3) «TPko::aS10
VAPJ48LE N MINIMUM MAAlMUM M£AN STU OEV
15«*C.NM 0
DESCRIPTIVE MtASUwt^ <10u> U*Y:O»CAT: (•<
VAPIA8LE N MINIMUM MAXIMUM MtAN STO OEV
15.rlC.NM UXY!3«CAT: (•«»)
VAPIA9LE N MINiMUM MAAiMUM M£AN STO OEV
15.*C..MM Z ,2bOOu -1 . OXY :b»CAT : ( *u) 'T^^O : 55 1 J
VAP[A8Li N MlNlMvJM ^AAi^UM ^ JAY : 3»CAT : ( »^»
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15.rtC.NM
DESCRIPTIVE «£
VAPIA8LE
IS.rtC.NM
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2 .27100
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2 .5i70u .b3<»00 .52550
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2 .6lbOu .&5600 .63550
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VAPJA8LE N MINIMUM MAXIMUM M£4N
15.HC.NM 2 .SJUOO . .S650U .b*.7SO
VAPI481.5
15.rtC.NM
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VABIA3L?!
15.rtC.NM
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UXY : 3«CAT : ( • n »TP4u : SSI U
N MINIMUM MAXIMUM MEAN"" STO DEV
2 .scuuu -1 .seOOO -1 .56000 -1
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DESCRIPTIVE ME4SUHES OXT : 3«CAf : t «a) •TfrfO: SS10
VARIABLE N MINIMUM MAXIMUM M(£AN 5TO 0£V
15.rtC.NM 'i. .21600 .33470 .37535 .22S3b
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IS.rtC.NM ' 'JAY : 3»CAT : ( « 1 ) 'Ti-rtO : SS20
VARIABLE N MINIMUM MAXIMUM MfcAN 5Tu OEV
15.rtC.NM 3 .50000 -2 .JOOOO -1 .15000 -1 .16<»64 -1
DESCRIPTIVE «£AsUr(6.S UXY:h»CAT: ( « 1 ) »TP^O: iS20
VAMIA8LE N MINIMUM MAXIMUM MEAN STU OEV
1S.MC.NM 2 .'.oOOO -2 .<»OOOU -2 .*0000 -2
DESCRIPTIVE M£4SUH£s OXY :o«CAT: («2> »THHU:SS20
VAPIA8LE N MINIMUM MAXIMUM MfcAN STU OEV
15.nC.NM 2 .boOOo -2 .fUOOu -£. .00000 -2 .1<*1*»2 -2
15.rtC..NN; 1 . /-j'lov -s . /uOOu -i ./OOuO -2
DESCRIPTIVE MtASUK£s Ox Y : 0«CA T : ( « 3 ) « THKO : 332u
VAPIAHLE N MINIMUM MAXIMUM M£AN STU OEV
15.nC.NM 1 .70000 -2 .70000 -e .70000 -2
UXY :3<>CAT: ( * j) »Ti-Mu:sS20
VA>".4HLE N Mlf.'lMUM MAXIMUM M£4N aTO OEV
-------
5-63
15.rtC.NM
OESCHIPTIVE.
VA»IABLE
15.HC.NM
DESCRIPTIVE
j .dUUOO -i .C3000 -1 .UJ33 -1 .77675 -2
OXY:3«CAT: ( ».)) »TP*Q: SS20
N MINIMUM MAXIMUM *tAN STO
<1JO> Ox Y : 0»CAT :(«<»> »TP*0: SS20
MINIMUM MAAlMUM NtAN STO OEV
1 . liflOV) .12HOO .12MUO
UXYO'CAT: I •<.) »T?KO: SS20
MINIMUM MAAlMUM MEAN STU OEV
«! .3<»000 -1 .iiOOO -1 .^abOO -I .U021 -1
15.DC.NM
OtSCWIPTIvE
VAWIAHLE
DESCRIPTIVE -EASUH&S <1J«> OXY:S»CAT: ( •<») «TPKO:SS20
VAWU8LE N MINIMUM MAXIMUM MtAN aTU OEV
15.HC.Nf 1 .3 UXY :o*CAT : ( »a) »Tfntu:SS2u
N MINIMUM MAXIMUM MtAN STU OEV
15.MC.NM
OESCHIPTIVE
VAPIA8LE
15.rtC.NM
VE "E
UX Y : 3*CAT : ( «5>
N MINIMUM MAXIMUM
M£AN
STU OEV
2 .-o^OO
. -.bsOu
DESCRIPTIVE MEASURES <13e> UAY : 0«CAT : ( «b) »TP«<0: SS20
VAP[AHl_E N MlNiMUM MAXIMUM MEAN
15.nC.NM t
3T'J D£V
,joOo2 -i
STU UEV
.J677U -1
DESCRIPTIVE
ux Y : 3»CAT : ( «o *
-------
5-64
VARIABLE
15.HC.NM
N MINIMUM
MAXIMUM
MEAN
.51600
DESCRIPTIVE MEASURES <13»> OXY:S»CAT:(*o)«TP«0:SSdO
VAPU3LE N MINIMUM MAXIMUM M£AN
1S.MC.NM 2 .4JVOO .<»6500 .^5200
STO OEV
.JlllJ -1
STU UEV
.Ib3a5 -1
DESCRIPTIVE M£4SUrt£? <13v> UAT : 0*CAT: ( «7)
VAPIA8L: N MINIMUM MAAl^UM
15.MC.NM 3 .26000 -I .16200
DESCRIPTIVE
15..HC.NM
15.rtC.NM
DESCRIPTIVE
VARIABLE
15.MC.Ni-;
DESCRIPTIVE -
VARIABLE
15.-1C.-NM
DESCRIPTIVE «
15.nC.NM
l v£
: SS20
MgAN STO 0£V
.81667 -. .71276 -1
OXY : j«CAT: ( «7) «TPKO: SS20
MlNlMUN MAXIMUM ,«CAN iTD 'JE V
2 .7UOOO -1 .11200 .^1000 -1 .<:9e>9d -1
STU U£V
OXY:S»CAT:
N MINIMUM MAXIMUM
1 .UJOO .U300
MtlN
.12300
OXY :o«CAT: (»e) »TPHO:SS20
MINIMUM MAXIMUM M£AN
2 .27^70 .31900 .2S935
<1-*J> OXY: 3«CAT: (»•>) «TP*u:3S20
. MINIMUM MAXIMUM M£A*
: S520
STO 0£V
.27789 -1
STD 0£V
: 0«CAT :.NO^t
MINIMUM MAAi^UM
7 .3jdOO .-'/20o
MINIMUM MAXIMUM
.J3200
S TO 0£V
.<»0<»33 -1
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-------
5-65
DESCRIPTIVE MEASUKES OXY :S»CAT :NONt«TPr<0: SS20
VAPIA8LE N MINIMUM MAAIMUM M£AN
15.HC.NM 0
DESCRIPTIVE
DESCRIPTIVE -
1S.MC.NM
OtSC»IPTlv£
VAPJAStE
15.MC.NM
DESCRIPTIVE
VA»IAfiU£
1S.HC.NM
DESCRIPTIVE
VARIABLE
STu DEv
OXY:O»CAT :SToC««Tii'HO:sS20
N MINIMUM MAXIMUM M£AN 5TO OEV
3 .10000 -2 .30000 -2 .23333 -2 .*30*<» -2
<15l> u*Y : u«CAT : ( »1 ) «TPHO : SS30
N MINIMUM MAXIMUM I£AN 5.ru OEv
2 .10000 -2 . OXY :b«CAT : ( « 1 ) »TPh(0:SS30
N MINIMUM MAXIMUM M£ 4N STu OEV
'd .*.oOOu -2 .iOOuo -H .<*iOOO -2 .70711 -3
OXY : 0«CAT : ( «i) »TMHO: SSJO
N MINIMUM MAXIMUM *tAN ^T^ OEV
2 .-OOOo - UX Y : b»CAT : I *t ) «TP^O : SS30
N MlMiMIJM MAA i «I.;M '-'Ir.iN alj DEV
1 .7uOdu -< ./OOOo -i .?0000 -2
VAHU8LE N MINIMUM
15.MC.NM 1 .^UOOO - UXY: j-
'- MINIMUM MAA!M-JM
MAXIMUM Mfc.AN bTQ OEV
.*OOOU -2 .-^0000 -2
STu Otv
-------
5-66
15.MC.NM
DESCRIPTIVE
1S.MC.NM
j . 1*000 -1 .33000 -1 .32b67 -1
UX Y :5»CAT s < « J) »TH*0: SS30
N MINIMUM MAAlMUM M£AN
U
-1
STU OEV
OXY :o»CAT :<»<») «1>|<0:SS30
MINIMUM MAXIM.JM < M&AN STU OEv
15.HC.MM 1 .10UOO -1 .1UOOO -1 .10000 -I
DESCRIPTIVE M£ASUW£s ox Y : 3»C*T : ( <•<•> *TPnu: SS30
VA^lAdtE N MINIMUM MAXIMUM Mfc.4N STL) UtV
15.nC.NM i .6UOOO -2 .oOOOO -2 .60000 -2
OESCHIPTIvE
15.nC.NM
VASIA&L.F
15.rtC.Nf-i
OESC«IPT!v£
VAWIA9I..E
15.-iC.NM
N MINIMUM MAXIMUM M&AN STO OEV
1 .7UUOO -2 .70000 -2 .70000 -*
UXT:O»CAT: («
N MINIMUM MAAlMUM MfcfiN 5TU OEV
1 .6JOOU -1 .aJOOO -1 .eJOOO -1
OAY:3»CAT: («5) »Tf»KO:SS30
N MINIMUM MAXIMUM M£4N STU OEV
1 .U200 .1)200 .13200
5TU OEV
OXY :^»CAT : ( a}) «TP*0 : SS JO
lNi MINIMUM MAXIMUM ^£iSN
-2
<16o> OXY : 0«CAT : ( «6)
N MINIMUM MAXIMUM
e. .3*000 .J*r0u
SS30
M&AN
JS'J'sO
3 fU J£V
-2
x Y : 3»CA T :
S"530
-------
5-67
VAPIA8LF
15•HC.NM
DESCRIPTIVE -i
VABIA8LE
15.MC.NM
DESCRIPTIVE «
VARIABLE
15.HC.NM
STO 0£V
15.MC.NM
DESCRIPTIVE
15.MC.NM
OESC«lPTIv£
VAWIA8I.E
15.HC.NM
DESCRIPTIVE
15.rtC.Ni-i
STu 06.V
N MINIMUM MAXIMUM MgAN
a .40500 . <*ot OXY:5»CAT:(«o)
N MINIMUM MAXIMUM MtAN
2 .2ttbOO .30800 .32650
UXY :o«CAT: (»7) »Ti|>HO:SS30
N MINIMUM MAXIMUM M£A(J STlj UEV
± .4UOOO -
N MINIMUM MAAl^UM MEAN STO U£V
2 .*UOOO -2 .30000 -2 .^»SOOO -2 .70711 -3
<171> UXY:S»CAT: (»7)*TPKO:SS30
N MINIMUM MAAlMUM MtAN 5TD
1 .50000 -2 .30000 -«i .50000 -2
STD OEV
.d2731 -2
5TD OEV
OXY:O*CAT: (»
N MINIMUM MAAlMUM MtAN
2 .21700 .22H70 .22285
<17j> OXY : 3»CAT : ( «d) «TPHO: SS30
N MINIMUM MAXIMUM MtAN
MtAiuKtS
15.nC.NM
Oxr ;
I . Jj<»uc
^ T INONC^T^KO : 5S 30
,jo<.oo
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MINIMUM
S:D OEV
.17^31 -I
aTU Utv
-------
5-63
DESCRIPTIVE
VAPIA8I.S
15.HC.NM
<177> OAY : S«CAT :NQNt»TPHO : SS30
N MINIMUM MAXIMUM M£AN
0
STO OEV
DESCRIPTIVE M£ASUK£S OA Y : O'CAT : STOCK'THKu : SS.30
VARIABLE N MINIMUM MAAlMUM MEAN STO OEV
15.MC.NM <• .2uOOo -2 .aOOOU -2 .J2SOO -2 .15000 -2
DESCRIPTIVE "
VARIABLE
' 15.MC.NH
VAOIA8LE
I5.MC.NM
VAMIASLE
1S.HC.NM
< OXT : 0»C4r:NOiNlt»TPMC:ss<»0
N MINIMUM MAAlMUM M&AN
i. .30SOO .J2«00 .JUOO
OXT : 3
MiNlMUM MAAlMUM
1 .28VOO .^8900
MgAN
.2^900
MINIMUM
MAXIMUM
MEAN
STU OEV
-1
STO OEV
STu U£V
DESCRIPTIVE M£ASU*tS < OXY : O'CAT : SJ
VASIA3LE N MINIMUM MAXIMUM MEAN STD OEV
IS.riC.NM - u. .JUOOu -2 .17500 -2 .125B3 -2
-------
i NUMIIt K
UNiVtHbllY Of MlllllliAN ItHMlNAL SYSTEM (MODEL AH I 7 J >
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WED MAY 11/83
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-------
NUMHCR
UNlVEHSIlr Oh MICHIGAN IEHMINAL SlTSlEM (MOOLL A»O73)
U:5B<44 EOT
1HU MAY
MMMMM MMMMM
MMMMMM MMMMMM
MMMMMMM MMMMMMM
MMMMMMMM MMMMMMMM
MMMHMMMMM MMMHMMMMM
inn
inn
mil
HMMMMMMMMM KMMMI-IMMMMM
M.1MMM
MMMMM
HMM'-IM
MMMMM
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MMMMM MMMMM MMMMM
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MMMMMM MMMMM MMMMM
MMMMMMMMM MMMMM
MMMMMMM MMMMM
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ssssssssssss
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sssssss
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sss
444
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44 44
44 44
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NN NN NN HHHHHHhHHHHh 444444444444
NN
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NNNN MM HH
NNN HH HH
NN HH |IH
M HH HH
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-------
IDAS
AIISIICA1. RtSEAHCn LAUOHAIOHt
E UHIVfHSlTY OF MICHIGAN
:SH«2l
Y 12, 1483
r AO F II e =-l < 1001 ) VAH=lt,10.ll,12.13»l<«»lS,16 L AbEL=NUMB£f
-------
BYSJHAIA
tSCHIHllvt MEASUKts OXYOUCAI s («/)
VA^iAtnt
9.ALDY
lO.Ml'd
11. MC
12. CO
K.NOX
IS.rtC.NM
l6.Mt rtlANOL
N MINIMUM MAAlMUM
A lO^.lC IOb.8^
2 1 J.oJd 1J.//0
i , \
-------
APPENDIX 6
Unscheduled Maintenance
on the Vehicle
-------
Date
Aug. 06, 1982
Aug. 10, 1982
Aug. 18, 1982
Oct. 26, 1982
Nov. 02, 1982
cfov. 04, 1982
Appendix 6
Unscheduled Maintenance on
Problem
Fuel pump failure
Ran out of fuel
None
Stalls shortly after
cold start
Fuel guage inoperative
None
Nov. 08, 1982 Starter wouldn't disengage
Nov. 10, 1982
Nov. 19, 1982
None
High thermocouple reading
in catalyst (over 1600°F)
Dec. 02, 1982 Emissions change (NQx)
Dec. 07, 1982
Dec. 08, 1982
Feo. 07, 1983
Apr. 13, 1983
Vacuum line to distributor
found disconnected
None
NQx change
None
the VW Rabbit
Repair
Replaced with pump from
local VW dealer
Refueled (no catalyst on
the vehicle)
New methanol-protected fuel
pump installed
Replaced thermal switch,
distributor cap and rotor
Replaced sending unit
(Nov. 8)
Hooked up digital idle
stabilizer, per VW
instructions.
2 relays interchanged by
local dealer, old thermal
switch installed
New thermal switch
reinstalled
Inspect catalyst, recorder
malfunction
Fuel pump from dealer re-
installed for diagnostic
purposes
Reconnected vacuum advance
hose
Methanol-protected fuel
pump reinstalled
New 02 sensor
New battery installed
-------
APPENDIX 7
Steady State Data at .
0, 10, 20, and 30 Miles
per Hour
-------
Summary of the Idle Test Results
with Operation as 3-Way Catalysts
Catalyst
None
5 L't: Uh (40)
12 L't: Kh (40)
12 I't: l
-------
Suiimary of die Idle Test kesults
with Operation as Oxidizing Catalysts
Catalyst
None
5 Pt: l
-------
Suinnary of the Idle Test Results
with Operation as Oxidizing Catalysts
Catalyst
None
5 Ft: Uh (40)
12 Ft: Uh (40)
12 Ft: Kh (40)*
3 Ft: 2 Fd (20)
Fd (40)
Fd + UM (35)
Cu
Fd (20)
Ag (150)
Oxygen
Level
/ Q V
(*)
5
5
5
5
5
5
5
5
5
5
IIC
.10
N/A
.00
.00
.05
.01
.14
.16
.02
N/A
NM1IC
N/A
N/A
.00
.00
N/A
.01
.13
.16
.02**
N/A
Methanol
— (g/roin) ~ •
.30
N/A
.00***
.01
N/A
N/A
N/A
N/A
N/A
N/A
CO
.75
N/A
.00
.01
.00
.01
.62
.62
.00
N/A
NOx
.01
N/A
.01
.02
.02
.02
.04
.03
.02
N/A
Aldehydes
(mg/min)
19.6
N/A
1.0
1.5
53.0
28.0
N/A
N/A
123.0**
N/A
Riel
Min
CjciJ-
120
N/A
122
119
116
118
120
115
121
N/A
Number
of
*TVv<-»Vj-»
IcSCS
2
0
3
1
2
2
2
2
2
N/A
N/A means data are not available
*Kacetrack, others are round
**based on 1 test
***based on 2 tests
~-J
I
-------
Suiiiitary of the Test Data at 10 Miles per Hour with
3-Way Catalyst Operation
Catalyst
5 Pt: Kit (40)
12 Pt: Kh (40)
12 Pt: Kit (40)*
3 Pt: 2 Pd (20)
Pd (40)
Pd + UM (35)
Cu
I'd (20)
Ay (150)
Oxygen
Level
0
0
0
0
0
0
0
0
0
0
HC
.48
N/A
.02
.02
.03
.10
.28
.65
.17
.24
NMitC
.45
N/A
.01
.01
.03**
.06***
.27
.64
.15
.23
Metnanol
(g/nu)
1.05**
N/A
.03
.16**
N/A
.52**
N/A
N/A
N/A
N/A
CO
3.08
N/A
.00
.00
.19
2.89
5.16
7.81
2.22
6.67
NOx
.32
N/A
.03
.23
.04
.03
.29
.31
.03
.30
Aldehydes MFC
(mg/mi)
144.6
N/A
1.0
1.1
N/A
26.2
75.7
N/A
N/A
N/A
10.00
N/A
10.05
10.35
10.00
9.77
10.30**
10.10
10.10
10.05
Number
of
Tests
5
0
2
2
2
3
2
2
3
2
N/A means data are not available
*Kacetrack, others are round
**based on 1 test
***based on 2 tests
-------
Summary of the Test Data at 10 Miles per Hour
with Oxidizing Catalyst Operation
Catalyst
None
5 Pt: Kh (40)
12 Pt: i
-------
Summary of the Test Data at 10 Miles pec Hour
with Oxidizing Catalyst Operation
Catalyst
None
5 Pt: Kh (40)
12 Pt: Uh (40)
12 Pt: l
-------
Suinnary of the Test Data at 20 Miles per Hour
with 3-Way Catalyst Operation
Catalyst
None
5 Ft: Hh (40)
12 Ft: l
-------
Summary of the Test Data at 20 Miles per Hour
with Oxidizing Catalyst Operation
Catalyst
None
5 ft: l
-------
Summary of the Test Data at 20 Miles per Hour
with Oxidizing Catalyst Operation
Catalyst
None
5 t>t: Kh (40)
12 l>t: Kh (40)
12 Pt: Mi (40)*
3 Pt: 2 M (20)
W (40)
W + EM (35)
Cu
W (20)
Ag (150)
Oxygen
Level
(%)
5
5
5
5
5
5
5
5
5
5
HC
.34
N/A
.01
.01
.14
.04
.44
.46
.09
N/tt
NMHC
N/A
N/A
.00
.01
N/A
.03
.43
.45
.12**
N/A
Methanol
— (g/mi)-
1.19
N/A
.00**
.10
N/A
N/A
N/A
N/A
N/A
N/A
CO
4.37
N/A
.00
.01
,.16
.02
4.30
3.74
.01
N/A
NOx
.43
N/A
.47
.47
.40
.37
.43
.45
.41
N/A
Aldehydes
(mg/mi)
105.0
N/A
1.4
1.5
155.2
138.9
N/A
N/A
N/A
N/A
Number
MPG of
Tests
19.00
N/A
19.40
19.40
18.40
18.60
19.05
19.25
19.30
N/A
up to
2
0
2
1
2
1
2
2
3
0
N/A means data are not available
*Kacetrack, others are round
**based on 1 test
10
-------
Summary of the Data at
30 Miles per Hour with 3-Way
Catalyst Operation
Catalyst
None
5 Ft: Kh (40)
12 Ft: Kh (40)
12 Ft: l
-------
Summary of the Data at
30 Miles per Hour with
Oxidizing Catalyst Operation
Catalyst
None
5 Pt: l
-------
Summary of the Data at
30 Miles per Hour with
Oxidizing Catalyst Operation
Catalyst
None
5 Pt: l
------- |