EPA/AA/TDG/92-06
                         Technical Report
              Conversion of Methanol-Fueled 16-Valve,
            4-Cylinder Engine To Operation On Gaseous
                 2H2/CO Fuel - Interim Report IV
                                by
                        Ronald M.  Schaefer
                         Fakhri J.  Hamady
                         James C. Martin
                          September 1992
                              NOTICE

     Technical  Reports do  not necessarily  represent  final  EPA
decisions or positions.    They are intended to present technical
analysis of issues using data which are currently available.  The
purpose  in the  release  of such  reports is  to facilitate  the
exchange  of  technical  information and to  inform the  public of
technical developments  which  may  form the basis  for  a final EPA
decision, position or regulatory action.

              U. S. Environmental Protection Agency
                   Office of Air and Radiation
                     Office of Mobile  Sources
           Regulatory Programs and Technology Division
                   Technology  Development  Group
                        2565 Plymouth  Road
                       Ann Arbor, MI  48105

-------
       UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

                    ANN ARBOR. MICHIGAN 48105

                        JAN  8 1993
                                                        OFFICE OF
                                                     AIR AND RADIATION
MEMORANDUM
SUBJECT:  Exemption From  Peer  and Administrative  Review
FROM:
Karl H. Hellman, Chief
Technology Development Group
TO:
Charles L. Gray, Jr., Director
Regulatory Programs and Technology Division
     The attached  report entitled "Conversion of Methanol-Fueled
16-Valve, 4-Cylinder  Engine  To Operation On Gaseous 2H2/CO  Fuel -
Interim Report IV," (EPA/AA/TDG/92-06) describes progress to date
on a project to convert a Nissan CA18DE engine previously modified
for operation  on M100 neat  methanol  to  operation on  dissociated
methanol (2H2/CO) gaseous fuel.  This engine was operated on both
M100 and simulated dissociated methanol (67 percent hydrogen and 33
percent  carbon monoxide)  fuels.   This   report  describes  recent
modifications  made to  the engine  and  fuel  delivery  system  and
summarizes the results from  recent testing.

     Since this report is concerned only  with the presentation of
data and its analysis,  and does not involve matters of policy or
regulations, your concurrence is requested to waive administrative
review according to the policy outlined in your directive of April
22, 1982.
Concurrence:
 larles L. Gray,/Jr/, Director, RPT

cc: E. Burger, RPT
                                     Date:

-------
                        Table of Contents
                                                          Page
                                                         Number
I.   Summary ..... 	 	 1
II.  Introduction	2
III. Description of Test Engine	2
IV.  Recent Fuel System Modifications	4
V.   Exhaust Measurement Procedure 	 5
VI.  Discussion of Test Results	6
     A.   simulated Carbureted Operation 	 6
     B.   Simulated Direct Injection Operation 	 8
     C.   Emissions and Combustion Analysis	11
VII. Summary and Conclusions	 .20
VIII.Future Efforts	20
IX.  Acknowledgments	21
X.   References	21
APPENDIX A - Test Engine Specifications	A-l

-------
I .
     A 16-valve, 4-cylinder light-duty automotive engine has been
converted to  operation on a mixture  of  hydrogen (H2)  and carbon
monoxide (CO)  gaseous fuel in a 2:1 molar ratio of H2 and CO.  This
engine has  been used  to investigate the  difference in emission
levels and  power output between two  different  fuels:   M100 neat
methanol and simulated dissociated methanol gaseous  fuel (2H2/CO) .

     This report contains test  results of power output from several
engine/ fuel system modifications.  These modifications were made in
an attempt to increase the brake specific power output of the test
engine when operated on 2H2/CO fuel  in reference to M100 levels.
With   the   gaseous   fuel,  several   intake  port/ fuel   system
configurations and  fuel injection nozzle  designs were evaluated.
These modifications were evaluated to determine the effects of fuel
pressure, injection  location,  and fuel delivery methods on engine
performance .

     Gaseous  fuel  was delivered  to  the  engine  by  two different
methods,  premixed  air /fuel mixture  in  the  intake  manifold from
continuous  port injectors  (simulated carbureted operation)  and
simulated  direct  injection.     The   simulated  direct  injection
operation was achieved by inserting blockages in four of the intake
runners where the M100 fuel injectors were located.   As a result,
gaseous fuel was supplied through one intake valve and air through
the second intake valve.

     The largest torque achieved  in  this  evaluation with  2H2/CO
fuel was 80 ft-lbs,  approximately 80 percent of the maximum torque
levels obtained with M100 fuel  at the same WOT, 2,000  rpm operating
conditions.   This  torque was  obtained  in the  simulated  direct
injection configuration.  When  operating with the premixed mixture,
output  torque  reached  approximately 60   ft-lbs  with  frequent
abnormal combustion  occurrences,  most notably preignition  in the
intake manifold.  Preignition of a hydrogen containing fuel is not
an unusual occurrence. [1-5]

     Brake-specific  emission  levels  with  gaseous   fuel  testing
conducted in this most recent  evaluation were significantly lower
than levels obtained previously.  However,  engine-out  CO  levels
were approximately double the  level  obtained with M100 fuel.   HC
levels with 2H2/CO fuel operation were very low.

     Proposed future efforts  will utilize a mixture of M100  and
2H2/CO  fuel  for engine operation.  Emissions,  fuel consumption, and
engine performance will continue to be monitored for operation on
this mixed fuel.

-------
                               -2-


II.  Introduction

     With  recent  advances  in  internal  combustion  engines  and
emission control development, new technologies are being directed
toward improving combustion efficiency,  multi-fuel capability, and
reduced emissions.  Recent developments in engine technology' have
enhanced  stable burn  and  reduced emission  levels.   The  use of
various alternative fuels is also being  addressed to satisfy clean
air legislation for the 1990's.

     One alternative fuel candidate is the concept of using exhaust
waste heat to provide the energy necessary for the dissociation of
methanol  (CH3OH) to hydrogen and carbon  monoxide. Methanol may be
catalytically  decomposed  to H2 and  CO  gases  according  to  the
reaction:

     CH3OH(l)	2H2(g) + C0
-------
                              -3-
two intake  and  two exhaust valves per  cylinder.   The valves are
operated by dual-overhead  camshafts,  one each for the intake and
exhaust sides.

     The test engine was initially modified  by Nissan to better
utilize the qualities of M100 neat methanol over unleaded gasoline.
These  modifications  were  discussed  in  detail   in   an  earlier
paper.[6]  A summary of the test engine  specifications  when fueled
with M100 neat methanol is  included in  this report as  Appendix A.
     EPA  then  modified  this  engine  for  use  with
simulated
33 volume
dissociated  methanol fuel  (67 volume  percent H, and
percent  CO) .    The first modification  was the  installation,  at
Nissan's request,  of a  thicker head gasket.  This thicker gasket
raised the clearance  between the valve  face and the piston crown;
this modification was made to improve the durability of the engine.
This  thicker gasket  lowered the  compression  ratio  from 11.0 to
10.5.

     With M100  fuel, the engine utilized  a 4-valve per cylinder
valvetrain configuration (two  intake and  two exhaust valves per
cylinder).  This arrangement was modified to allow for admission of
air  to the  cylinder through  one  intake valve only;  the second
intake valve supplied  the  2H2/CO  fuel.  The exhaust side valve
scheme was not altered  (Figure  1).  This  configuration is  hereafter
referred to as  simulated direct injection operation.

                             Figure 1

               Simulated Direct Injection Operation
                 Valve  Scheme For 2H-»/CO Fuel  Use
     This  valve scheme allowed for the admission of  gaseous  fuel
 only  through one  of the  intake  valves.   An intake air  control
 assembly encloses  the swirl control valves and is situated between
 the intake manifold  and the combustion chambers on the MIOO-fueled

-------
                               -4-
engine.  This assembly controls the air flow so that  it is through
one intake runner and/or through both intake runners  as necessary.
This is to control in-cylinder charge motion on the  liquid-fueled
engine.

     When the engine  was converted by EPA to operation on  2H2/CO
fuel, the control  valve slide and actuator were disassembled and
the swirl control  valves removed.   The runners through the valve
assembly that contained holes for the fuel injectors were welded
shut approximately 1/2-inch upstream from the holes.  These seals
prevented the  admission  of  air to  the ports through which the
gaseous fuel passes.  The holes in the assembly left by the power
valve slide were sealed to prevent leakage  of fuel and air between
runners.

     Fuel injectors were not used to deliver the 2H2/CO fuel.  The
rail and the individual injectors were removed and 3/8-inch inside
diameter stainless steel pipe fittings were used in their place.
The stainless steel fittings were threaded and the insides of the
aluminum  injector holes were then  threaded to  adopt to  these
fittings.

IV.  Recent Fuel System  Modifications

     A fuel supply cylinder outside the test cell was used with 22
feet of 1/4-inch stainless steel tubing leading from the pressure
regulator on the  cylinder to the solenoid  valve  inside  the test
cell.   After the  solenoid valve,  the fuel delivery  system was
completely altered.  The fuel line leading  from the solenoid valve
to  a  Tylan  mass  flow  controller was  3/8-inch  in  diameter and
measured approximately 27 feet in length.  There were only slight
bends and no turns in  this fuel line so fewer pressure drops in the
fuel delivery system would occur.

     Approximately 12 inches downstream of the Tylan mass flow
controller was a pressure gauge that would measure fuel pressure to
the intake manifold.   Ten feet downstream of the pressure gauge was
another  solenoid  valve  followed  by  a 2-stage  hydrogen  flame
arrester.

     The cylindrical plenum used previously to distribute fuel flow
to each cylinder was replaced with a 1/4-inch diameter fuel rail.
The fuel rail would distribute the incoming fuel to each of four
flexible fuel lines 3  inches in length leading to the  fuel injector
ports.   The total length from  the intake  valves  to the  flame
arrestor was approximately 11 inches.

     The  four   fuel  lines  are connected  to  the same  threaded
fittings which  are screwed into the fuel  injection  ports  in the
valve control assembly.  The inside diameter of these  fittings
(previously 1/4-inch)  were replaced with different nozzle designs
in  an attempt  to increase  fuel  pressure  and  enhance the fuel
distribution.   Nozzle  openings  from  1/2  to 3 millimeters were
evaluated to determine the best operating condition.  The gaseous

-------
                              -5-
fuel is supplied to the combustion chambers by the opening of the
fuel valves when the blockages in the intake air control assembly
were present.    With these  blockages,  fuel  flow to  the engine
occurred through one intake  valve  and  air through the other.  In
the remainder of this  report,  operation in this configuration is
called simulated direct injection.

     Some testing was also conducted with these blockages removed
while  still  using the  same fuel  delivery fittings in  the fuel
injector location.  Because the fuel and air were premixed in the
intake manifold when operated in this configuration, this operation
was  called  simulated  carbureted  operation.    Different  nozzle
designs and fuel delivery locations within the  intake manifold were
also evaluated in this premixed method.

V.   Exhaust Measurement ProGed"****

     Both  dilute and  cylinder-out  emission  samples  were  taken
during this latest phase of testing.  Cylinder-out  samples were raw
emission levels (not diluted) and were taken for each cylinder from
the runner of the exhaust manifold  leading from the exhaust valves
to  the exhaust  pipe.   Dilute  emission samples  were  engine-out
levels and taken downstream of the exhaust manifold.

     Dilute engine-out samples were taken  as engine exhaust passes
from the exhaust pipe to a 2-1/2 inch diameter  flexible metal tube.
This tube  passes the  exhaust  overhead to a 6-inch  rigid tube
supported from the test cell ceiling. The rigid tube delivers the
exhaust to a Philco  Ford 350 cfm  constant volume sampler  (CVS).
Total  length  of  the  flexible   and   rigid   tube  sections  is
approximately 40 feet.

     A gaseous  sample line  has been  extended through  the cell
ceiling and connect the mechanical CVS with an electronic display
panel in the cell control room.  A fitting in the sample line at
the control room enables bag sampling at this point.  Analysis of
bag samples  was accomplished at a bank of analyzers  located in
another test cell.  Hydrocarbon (HC) emissions were measured with
a Beckman Model  400  flame ionization detector  (FID).   NOx level
determination was conducted on a Beckman model 951 chemiluminescent
NOx analyzer.   Carbon oxides  (CO,CO2)  were measured  by infrared
technique using a Horiba Model A1A23 infrared analyzer.

     Cylinder-out emission samples were taken for each individual
cylinder from four different taps in the  exhaust  manifold.   The
sampling lines led to a Hankison Model E-4GSS compressed air dryer
that cooled the  emission sample through an R-12  refrigerant at a
rate of 1,215 Btu/hr.   The suction  pressure of this  unit was 33
psig.  The emission sample was then collected  in a bag.  The total
length of  the  sampling  line  from the exhaust  manifold to the
collection bag was approximately 8 feet.

-------
                              - 6-


     The bag  samples were  then  taken to  another  location which
contained a Nicolet Rega 7000 FTIR system.  This system allowed for
the raw emission sample to be diluted to 10 percent  with balance of
nitrogen.  Because the specific volume of emission sample taken was
not known,  brake-specific  emissions could not be  calculated for
individual cylinders.

VI.   Discussion of Test Results

     A.   Simulated Carbureted Operation

     Simulated  carbureted  operation was  obtained  by mixing the
gaseous fuel and air in the  intake manifold.  This premixed charge
resulted from removing the blockages that were previously located
in one of the  intake  runners  for each cylinder. All of the test
results presented here  were obtained  at  steady speed (2,000 rpm)
with bottled 2H2/CO fuel.

     The first phase of testing described here evaluated the effect
of three different nozzle size openings in the stainless steel pipe
fittings used to deliver the  gaseous  fuel.  These  pipe fittings,
again, were located  in the  fuel  injector  holes  in the intake
manifold.   Different nozzle  designs were  fitted  in  the  pipe
fittings in an attempt  to  increase the  fuel  pressure and fuel
distribution in  the intake  system to  improve  torque, combustion
stability,  and emissions.

     The first  nozzle evaluated was  I/2-millimeter  in  diameter.
The  maximum  fuel  flow  rate  these  nozzles  would  allow  was
approximately 6.7  cfm.   At wide open  throttle (WOT) conditions,
operation here resulted  in  an  air/fuel ratio (A/F)  of 15.4.   The
engine would not run at this lean condition.

     The  second  nozzle opening utilized  was 1-millimeter  in
diameter.  The maximum fuel flow rate with these nozzles was 10.6
cfm,  resulting in  an A/F  of 9.7  at WOT,  2,000  rpm  operating
conditions. The maximum torque obtained during this testing was 37
ft-lbs.  After approximately 1-2 minutes of engine operation, the
premixed charge would  begin to  ignite  in  the intake manifold and
substantially decrease output torque.  This happened every  time the
engine was  operated.   The engine  ran smooth until engine oil
temperature  reached   approximately   140°F.     This  preignition
condition at  hotter engine temperatures  is  quite common when a
premixed hydrogen containing fuel is used.[1-5]

     The next nozzle  investigated here utilized a  1.5-millimeter
diameter opening with  a diffuser.   Figure 2  shows  a schematic of
two different nozzle designs using this size opening.  With these
nozzles, the engine was severely hindered by  preignition in the
intake manifold. This preignition occurred after approximately 1-2
minutes of operation once the  engine has warmed.  Also, the engine
could not be operated at WOT  conditions  during any testing here.
As  the throttle was  being slowly  opened,  there  was a  certain
maximum airflow that would allow for smooth engine operation.  When

-------
                              —7—
the throttle was opened above  this point  (increasing airflow),  the
engine  would experience  frequent preignition.  The fuel  delivery
pressure was approximately 60 psig during this testing.

                             Figure  2

                  Simulated Carbureted Operation
                  Nozzle Openings With Diffusers
                                                  1 mm
                 Flow

                1.5 mm
          (a) Single-Hole Nozzle
(b) 4-Hole Nozzle
     Table l below is a summary of test results obtained with the
single-hole  1.5-millimeter nozzle  openings at  2,000 rpm.    Spark
timing for this testing was set at 10°BTDC.
Table 1
Simulated carbureted operation
2H2/CO Fuel Operation, 2,000 RPM Conditions
Air Flow
(ofm)
38
25
20
25
32
35
15
Fuel Flow
(cf»)
13.9
11.7
10.3
10.3
10.3
10.3
13.9
A/F
Ratio
7.4
5.8
5.3
6.6
8.4
9.2
2.9
Torque
(ft-lbs)
60
25
41
44
45
45
52

-------
                               -8-
     The maximum torque obtained during this testing was 60 ft-lbs,
approximately 60 percent  of  the level obtained with M100 fuel at
2,000 rpm, WOT operating conditions.  The engine was also severely
hindered by preignition in the intake manifold during every test
conducted  in  this  premixed  combustion  method and could  not be
operated at WOT.

     The next phase of testing utilized a different location for
the  fuel delivery  pipe fittings  in the  intake  manifold.   The
gaseous fuel was now introduced in the intake manifold before the
partition of the intake runners.   Four holes were drilled in the
intake manifold before the partition that led to each intake valve.
Therefore, a premixed air/fuel mixture was delivered to each intake
valve.  Different nozzle sizes were also used during this testing
including  the use of the 4-hole nozzle.   However, testing in this
configuration did not  increase output torque and also resulted in
severe preignition in the intake manifold.  Again, this preignition
occurred after 1-2 minutes of operation.

     B.   Simulated Direct Injection Operation

     Because of the severe  limitations on engine performance due to
preignition in the  premixed  combustion method,  the  passageway
leading to the fuel intake valve was again blocked off.  The fuel
delivery  pipe  fittings  with the  single-hole nozzles  were  then
mounted in the  fuel injector holes where the M100 fuel injectors
would normally be located.  This configuration allowed for mixing
of the  air and fuel  only in the  combustion chamber;  therefore,
simulating direct injection fuel delivery.

     The original pipe fitting with a nozzle opening equal to the
fitting  inside diameter   (1/4-inch)  resulted  in   smooth  engine
operation with  a maximum torque of 58 ft-lbs  at an A/F ratio of
8.3.   The fuel delivery pressure measured here was 52 psi.

     The first  phase of testing conducted  here utilized nozzles
from the  previous  subsection.   The maximum fuel  flow attainable
with these nozzles varied substantially.   The largest fuel  flow
obtained was 9.9 cfm,  resulting in an A/F  ratio of 11.0 at  WOT,
2,000 rpm operating conditions.  The highest torque achieved during
this testing was 66 ft-lbs.  However, the engine was  still affected
by a slight preignition in the intake manifold.

     The nozzle opening offering  the best  results  here  was  a 3-
millimeter diameter opening with no diffuser.  This fuel delivery
configuration resulted in very smooth engine  operation  and the
highest output torque obtained to date with this engine is 80 ft-
lbs at 2,000 rpm, WOT operating conditions.  Although this is still
80 percent of the  output  torque obtained when using M100 fuel at
the same conditions, several literature sources suggest that this
may in  fact be the output limit when using dissociated methanol
fuel.[14,15]    These  literature   sources  quantify the  maximum
obtainable torque  when operating  on  dissociated methanol as 55
percent of the M100 level.  The 80 ft-lbs obtained with this engine

-------
                              -9-
in this configuration may be close to the maximum attainable output
torque at these  operating conditions with the gaseous fuel.  The
engine also ran very smooth,  and operation at WOT was  not hindered
by  preignition during  any test conducted during  this  phase of
testing.

     Several  other  operating  conditions  were  also evaluated,
including fuel delivery pressure measured after the Tylan mass flow
controller  and  before  the  hydrogen  flame  arrester.    Another
operating condition  that was varied was  spark  timing.  Figure 3
below  presents a curve fit for the maximum torque  obtained at
several different ignition timings.   All torque valves presented
here were maximum values and obtained at 2,000 rpm,  WOT conditions.
Fuel delivery pressure  here was held relatively  constant at  about
60 psig.  The  largest torque at these conditions seemed to  occur
with a spark timing of  5 degrees before-top-dead-center (5°BTDC).
                             Figure 3
                  CA18DE Engine, 2H2/CO Fuel
               Simulated Direct Injection Operation
          70
          60
          50
          40
            Torque (ft-lbs)
            1                     5

                       Spark Timing (degrees BTDC)

      2,000 rpm, WOT, 60 psig fuel pressure.
15
     The next variable operating condition investigated was fuel
delivery pressure.   This fuel pressure was  measured in the fuel
delivery system after the Tylan mass flow controller and before the
hydrogen flame arrester. Spark timing was set at 5«BTDC.

     The fuel pressure measured  here was increased by  increasing
the regulator pressure at the gas bottle.  Figure 4 below presents
the results obtained at  2,000 rpm and WOT conditions.

-------
                   -10-
                Figure  4
       CA18DE Engine, 2H2/CO Fuel
    Simulated Direct Injection Operation

  Torque (ft-lbs)
80
60
40
 39
58
75
95
                          60     65     70
                           Fuel Pressure (psig)

        2,000 rpm, WOT, 5BTDC spark timing.

     The maximum torque obtained during this testing was achieved
with a fuel pressure of 75 psig.  When the pressure was increased
above 75 psig, output torque seemed to taper off.   For example, at
a fuel pressure  of  95  psig, output torque reduced  to 72 ft-lbs.

     Table  2  below  presents all  the results  obtained  from  this
testing  in the  simulated direct  injection  configuration.    All
torque values presented were maximum.  The  nozzles used had the
single-hole, 3-millimeter diameter openings without a diffuser, and
all results were obtained at 2,000 rpm,  WOT operating conditions.
Table 2
Simulated Direct Injection Operation
CA18DB Engine, 2,000 RPM/WOT Conditions
Spark
Timing
(BTDC)
1
5
5
5
5
5
5
15
Fuel
Pressure
(psig)
58
39
58
60
65
70
75
60
Air
FlOV
(cfm)
33
30
37
37
39
37
37
37
Fuel
Plow
(cfm)
15.5
14.1
16.7
19.2
20.9
24.0
22.5
16.6
A/P
Ratio
5.8
5.8
6.0
5.2
5.1
4.2
4.5
6.0
Torque
(ft-lbs)
60
53
69
75
78
78
80
64

-------
                               ••11-
     Engine operation was kept near to stoichiometric (A/F ratio of
6.5)  for most of this testing.   Several literature sources again
suggest best  engine  performance  occurs at  or slightly  rich of
stoichiometric when operating on hydrogen fuel.[1-5]



     The largest torque obtained during the previous testing with
2H2/CO fuel was 80 ft-lbs (80 percent of the M100 fuel output) .  As
a  result,  emissions  and combustion  analysis  were performed at
similar operating conditions (A/F ratio of 4.5,  2,000 rpm, WOT, and
a fuel pressure of  75 psig).   The  A/F ratio  of 4.5 utilized with
the gaseous fuel was similar to the closed-loop  controlled M100 A/F
ratio of 4.7 at the same 2,000  rpm, WOT  conditions.  Table 3 below
details the operating conditions used for both fuels when emissions
samples were collected and combustion analysis was performed.
Table 3
Engine Operating Conditions: CA18DE Engine
Fuel
M100
2H2/CO
Speed
(rp«)
2,000
2,000
Throttle
Position
WOT
WOT
A/F
Ratio
4.7
4.5
Fuel
Pressure
(p»ig)
45
75
Air
Plow
(of*)
39
37
Torque
(ft-lbs)
100
80
     Cylinder-out emission samples were taken for each of the four
cylinders.  Two samples for each cylinder were taken when operating
on each fuel.   These were raw (not diluted)  emission samples and
were analyzed using an FTIR system. Each sample taken was collected
over approximately 4 minutes.

     Figure  5 below  presents cylinder-out carbon monoxide (CO)
concentrations when using either fuel.  The top bar represents the
CO emission concentration leaving cylinder #1 when operated on M100
fuel.   Similarly,  the bar  underneath that  represents the  CO
concentration  leaving cylinder #1 when operating  on 2H2/CO fuel.
These results are the average of two test runs and are presented in
parts per million (ppm).  Again,  these are  raw emission levels and
not diluted.

-------
                               -12-
                             Figure 5
            Cylinder-Out Carbon Monoxide Levels
Cylinder Number


      Cylinder #1



      Cylinder #2



      Cylinder #3



      Cylinder #4
                   '/////////////////////I,
                 0     5    10    15    20    25

                  Carbon Monoxide (ppm) (Thousands)

   2,000 rpm, WOT conditions.
     Concentrations of  CO when using the gaseous 2H2/CO fuel were
much  lower  than  when  utilizing   M100  fuel.     These  low  CO
concentrations, ranging between 590  ppm for cylinder #3 and 1/750
ppm for cylinder #4, seem to indicate that most of the 2H2/CO fuel
is combusting  and that very little  unburned fuel  is  resulting.
This was  not the case  in previous testing with  2H2/CO  fuel when
large amounts of unburned fuel  were  present in the exhaust.[6,13]

     From  this  figure,  combustion  stability  from  cylinder-to-
cylinder may also be investigated.   With M100 fuel,  each cylinder
is producing approximately equal  amounts of  CO.   The  largest
variance in cylinder-out CO levels occurs between cylinders #1 and
#2, where a 20 percent variance occurs.  However, when 2H2/CO fuel
is used, cylinder /3 produces a much lower amount of CO than the
three other cylinders.   For instance,  cylinders #3 and /4 differ by
66 percent in CO emission levels.

     Figure 6 presents results from methanol emission sampling for
the same testing described in  Figure 5.

-------
                              -13-
                             Figure 6
             Cylinder-Out Methanol Emission Levels
    Cylinder Number


          Cylinder #1
          Cylinder #2
          Cylinder #3
          Cylinder #4
                  01234

                      Methanol (ppm) (Thousands)

    2,000 rpm, WOT conditions.
     When   operating   on   the   gaseous   2H2/CO   fuel,    large
concentrations  of  methanol  emissions  were  produced in  each
individual  cylinder.   Also,  in cylinder #2,  levels of methanol
emission concentrations  when operating on  this  fuel were  higher
than MIOO-fueled levels.

     When operating on M100,  combustion stability with regard  to
unburned fuel in each cylinder was again very good.  The  largest
variance in unburned  fuel occurred  between cylinders  #2 and #3,
where a 26 percent difference  in methanol emissions occurred.  When
operating on the 2H2/CO fuel,  cylinder #3 levels  again varied from
the other three cylinders by a substantial margin.   However, the
largest variance between cylinders when excluding cylinder #3  is
only 17 percent.

     Table 4 below presents several other emission levels measured
during this same testing.  All levels are presented in ppm's except
for water vapor (H20)  and carbon dioxide (C02),  which are presented
in a percentage.

-------
                              -14-
Table 4
2,000 RPM/WOT Conditions, Simulated Direct Injection Operation
Cylinder-Out Emission Levels
Cylinder
Number
#1
#2
#3
#4
Average
Fuel
M100
2H2/CO
M100
2H2/CO
M100
2H2/CO
M100
2H2/CO
M100
2H2/CO
H20
<%)
12
17
11
14
10
11
11
13
11
14
CO
(ppm)
23,650
1,200
18,930
1,620
20,000
590
23,595
1,750
21,544
5,160
CO,
(%)
1.0
0.9
1.0
0.9
0.7
0.5
1.0
0.8
0.9
0.8
NOX
(ppm)
825
1,800
1,100
1,475
520
N/A
925
1,540
842
1,605
CH3OH
(ppm)
3,400
2,935
2,715
2,785
3,655
1,815
3,210
2,425
3,245
2,490
ECHO
(ppm)
60
7
45
5
45
4
40
5
48
5
N/A = Not available
     Formaldehyde  (HCHO)  emission  levels  are  much  lower when
operating   on   the  gaseous   2H2/CO  fuel   for  each  cylinder.
Formaldehyde levels  when the  2H2/CO  fuel  was used  were,  on the
average,  90 percent below  corresponding M100  levels  for each
cylinder.    However, emissions  of  nitrogen  oxides  (NOx)  were
substantially  larger when  the  2H2/CO  fuel  was used.    On the
average, NOx levels approximately doubled from M100 levels when the
gaseous fuel was used.

     Two overall dilute emission samples with each fuel were also
taken.   The  operating  conditions were again  similar  to those
described in Table 3  for this testing.  These diluted samples were
analyzed at a different  site using different analyzers.   Table 5
below presents the average of two emission samples when  operated on
each   fuel.     Brake-specific  emissions  are   presented  here
(grams/brake horsepower-hour).   Methanol  and formaldehyde levels
were not measured  during this testing, and only a total hydrocarbon
(HC) value is presented here.
Table 5
2,000 RPM/WOT Conditions, simulated Direct Injection Operation
Brake-Specific Emission Levels
Fuel
M100
2H2/CO
BhP
38.1
30.5
A/F
Ratio
4.7
4.5
HC
(g/BhP-hr)
1.37
0.03
CO
(g/BhP-hr)
24.7
49.0
NOX
(g/Bhp-hr)
2.0
8.0
C02
(g/BhP-nr)
205
450

-------
                              -15-


     HC levels when using the gaseous fuel were substantially lower
than  MlOO  levels  on a  brake specific  basis.   However,  brake-
specific CO levels approximately doubled from MlOO levels with the
2H2/CO fuel.   This level of CO  is  substantially lower, however,
than  levels  obtained  in   a  previous  report  [6]  and is  also
accompanied with a higher torque  of 80 ft-lbs.  Although NOx levels
with  2H2/CO fuel  were much higher,  these levels  are  similar to
previous NOx emissions.[6]

     The second phase  of testing in this subsection consisted of
investigating  the in-cylinder combustion process when utilizing
each  fuel.    This  investigation was conducted  using  a  Kistler
pressure sensor and the test  cell data  acquisition system.   This
investigation  was performed using a pressure versus crank angle
(CA) approach.  The computer software program then computes eight
other outputs based on the experimental pressure/CA diagram, engine
geometry, and operating conditions entered at the  beginning of each
test.  There  are  four  basic categories  of functions which result
from the further  analysis of the  pressure/CA  data.  These include
dynamic cylinder pressure and temperature data needed for a thermal
stress analysis,  heat  release rate  and  cumulative heat release,
cycle performance and losses from the indicator diagram, and cycle
thermodynamic data.[9]  This report will only  investigate pressure
and heat release  data.

     When operating on each fuel, pressure data was gathered from
each cylinder  individually.  However, data from each cylinder was
very similar; therefore, only one set of data for  operation on each
fuel will be presented in this report.  When MlOO  fuel was used, 25
consecutive cycles were monitored and averaged  by the computer.
With 2H2/CO  fuel,  fifty consecutive cycles were averaged. The same
operating conditions for each fuel,  presented in Table  3,  were
again used in  this phase of testing.  The maximum torque obtained
at 2,000 rpm,  WOT conditions  with MlOO  fuel was  100 ft-lbs,  with
2H2/CO,  it was 80 ft-lbs.

     Figure  7 below presents  in-cylinder pressure  versus  crank
angle data  when  using MlOO fuel.   The  maximum pressure obtained
with MlOO fuel reached 808  psi.   This maximum  pressure occurred at
approximately 7 degrees after top-dead-center  (ATDC).  Spark timing
with MlOO fuel was  22 degrees BTDC.  The indicated mean effective
pressure (imep) was calculated by the software to be  119.6 psi for
this fuel.  The standard deviation in maximum pressure values for
25 consecutive cycles was found to be 28 psi.

-------
                                 -16-
                              Figure 7

                   Pressure Trace With  M100 Fuel
           ECA
           901
ENGINE  CYCLE ANALYSIS
   FILE
637,MT
         B= 3.2   S: 3.2     I- 5.2    Ctel8.5

         SUN=25   T«st Oat«:86-88-92/14:17:11
                    R!*=1999.i    INEP: 119.6

                      Print Date:86-«8-92
         -880
         PS 14



         -488
         P - 9
                   ENGINE ID:
                   CA18DC
            PMJC= 886 at  6.99CA
               *
               ; \
-288 / \ '
-
-— —
-9
-98 TDC 98
': '• i 1 1 1 i i i 1
     A  similar trace was  obtained when the  2H2/CO  fuel  was used.
(Figure  8)   Maximum  pressure levels  reached with  this  fuel were
slightly lower than M100 fuel, at 754 psi.   This maximum pressure
was achieved at 14 degrees ATDC.  Spark timing with this fuel was
set at 5 degrees BTDC.  Although the maximum output torque achieved
with  2H2/CO fuel  is  approximately  20 percent  lower than M100
levels, the calculated  imep when using the gaseous fuel is about 20
percent higher.  The imep again is a calculated quantity derived
from pressure, engine geometry, and operating conditions data.  The
higher imep values with gaseous fuel operation may be attributed to
the following.  First,  the number of cycles used for M100 operation
was different  from that of  2H2/CO  operation, which may  alter the
software averaging process.   Also,  prior to 2H2/CO fuel operation,
the optical encoder was removed then remounted on the engine.  This
may significantly change  encoder position  and  consequently imep
measurement.   The  standard deviation  in maximum cylinder pressure
with 2H2/CO fuel was 14 psi, denoting  less fluctuation  and more
stable operation than with M100 fuel.

-------
                              -17-
                          Figure 8
                Pressure Trace For 2H->tCO Fuel
5£? i ENGINE CYCLE ANALYSIS j
; 901 ;j ,
B= 3.2 S: 3.2 i- 5.2 Ctelfl.S RP»fe2Wl,9
SU*=5« Test »at«: 98-31-92/13:22: 51 Print Da
|P - 9 j ENGINE If. PMX= 754 at 13.99O)
OU80E

-8M
psi* ft.
i \
-<» / \
/ \
\
1 \
i i
/ \
*400 ' \
\
/ \
/ \
/ \
V

-4
-99 TK >
ill i i I i i
MTU FILE :
331921. MT :;
IHE7= 144.2
t«:M-31-92 :
i

i
i

1
j
i
H
i
1
^
i

-i
i
i
1
J
i
	 	 -J
• , . \
     One possible way of investigating flame speed/ combust ion rate
is by  investigating  the heat release rate.    Recent literature
suggests  that this  quantity is  proportionally related  to mass
burned  rate  (energy  release) ,  with  only a  slight difference
involved, resulting  from neglecting the heat release through the
cylinder  walls and  blowby. [10,11,12]   The  software  uses this
quantity  because  it is  much faster to calculate a  rate of heat
release than a rate of combustion. [9]

     Heat release rate,  denoted dX/d6  is calculated  from cylinder
pressure/volume and crank  degrees data  by using  the following
formula [9]:
dX/d9 = [l/(92 -e,)][l/(n-l)][P2V2 -
                                         + (1/2) (P,  -  P2)(V2 - V,)
Where:
    dX/d0
     P

     V

     n
               Heat release rate between two crank angles
               (Btu/degree)

               Cylinder pressure (psi)

               Cylinder volume  (cubic inches)

               Polytropic index.

-------
                              -18-
The  maximum  heat  release  rate  (related  to mass  burned  rate)
obtained with M100 fuel was 0.035 Btu/CA.   Similarly,  the maximum
heat release  rate with the 2H2/CO fuel was 0.050 Btu/CA.

     From  the heat  release  rate  values,  it  is  possible  to
investigate  a combustion  duration.  This  duration period  can be
calculated  from  the cumulative  heat  release (cumulative  energy
release) versus crank angle data.  This quantity is proportional to
the amount  of chemical  energy which must  be released  as thermal
energy by combustion to match the measured pressure  data.

     Figure 9 below presents the trace of cumulative heat release
(denoted X) versus crank angle when M100 fuel was used.  The y-axis
here represents the fraction of the total heat released during an
average  of   25   combustion  cycles.     For  instance,   at  TDC,
approximately 30  percent of  the total heat  release when combusting
this fuel has  occurred.  The start  of combustion  has  been selected
as  X=0.05,   or when 5  percent  of  the  total  heat  release  has
occurred.  Similarly,  the end  of combustion has been  selected as
X=0.95, or when 95 percent of the total heat release  has occurred.
These  values  were  chosen based upon  the  recommendation of  the
software developers.[9]
                              Figure 9

              Cumulative Heat Release With M100 Fuel
            ECA
            9 a i
ENGINE CYCLE ANALYSIS j[
                         ;i   MT« FILE
                            632. MT
          ! B= 3.2   S: 3.2    L: 5.2   CJfclg.3
           SUN=23   Test D»tt:86-93-92/09:42:37
                   Wit 2982.3
                     Print 9»t«:96-9?-«2
          IX -
          -.7

          -.«

          -.5

          -.4

          -.3

          -.2

          -.1
 ENGINE i»:
 CA199C
                                                 .95
i ! •
1
31 M |
; i i i i i i i 1

-------
                              -19-
     The  total  heat  release  duration  (related  to  combustion
duration) was 85 crank degrees for M100  fuel.   Previously,  this
duration was  calculated to be approximately 60 crank degrees for
M100 fuel.  However, with the shorter combustion duration, measured
output torque was much higher (128 ft-lbs)  than the level measured
during this testing  (100 ft-lbs).  It was not determined why output
torque dropped off  from levels obtained  during  previous testing
with M100 fuel.[13]  The heat release trace here reveals a fast-
burn rate until approximately 70 percent of the total heat release
has occurred.  After this point, the heat release rate appears to
be very slow  and prolonged.

     Figure  10 below  presents a  similar trace  for  2H2/CO  fuel
operation.   The total heat  release duration  with this  fuel was
approximately 63 crank degrees, substantially faster than the M100
results.  A faster  burn rate would be  expected with  a hydrogen-
containing  fuel.    At  20  crank degrees after  spark,   (15°ATDC)
approximately 80  percent of  the combustion has occurred.   Eighty
percent of  the total combustion  was  not reached until  60 crank
degrees after spark with M100 fuel.    The total amount  of  heat
released during one combustion event with the 2H2/CO fuel was 0.84
Btu.   The  corresponding value  with  M100  fuel was  0.63  Btu,
approximately 25 percent lower.

                             Figure 10

             Cumulative Heat  Release With 2 Ho/CO Fuel
            CCA
            90J.
ENGINE CYCLE ANALYSIS

        9ATA FILE :
        831922. MT
          B= 3.2   S= 3.2    L= 5.2    Cfcli.5
          StHtSB   Test Bate:88-31-92/13:23:16
                   RPIt28tt.3

                     Print Date:88-31-92
          X - *
 ENGINE ID:
 CA18K
X(1MK>= .84 BTU
          -1

          -.9

          -8

          -.7

          -.4

          -.3

          -.4

          -.3

          -.2
                                     J

                                     1

                                     4
                                    J
                                     4
                     .85

                     TDC
             38
              i
     M
      i

-------
                               -20-
VII. sunnnaT-v and Conclusions

     This  engine  conversion  project  was  started  to  develop a
suitable test  bed  for a practical on-board methanol dissociator.
From the  engine performance,  the following main results can be
summarized:

     1.   The  engine  currently operates  smoothly  on dissociated
methanol fuel at approximately 80 percent of the M100 output power
level.  This power output is considerably higher than the maximum
power levels reported in another  literature source  [14], when the
engine operated on 100 percent dissociated methanol.

     2.   In premixed combustion,  the  engine  must  run  on a lean
mixture.  Abnormal combustion  is likely to occur when the engine
warms up.  This is considered to  be a restriction on the range of
dissociated methanol operation.

     3.  The standard deviation in maximum cylinder pressure with
the 2H2/CO fuel is less than M100 fuel deviation.  This indicates
less fluctuation and more stable engine operation with the gaseous
fuel.

     4.   Dissociated methanol  burned  much faster  than methanol
probably resulting from the hydrogen content in the fuel, which has
a flame speed over five times that of methanol (see Figures 9 and
10) .

     5.  The lower efficiency with dissociated methanol  (as is the
case with any gaseous  fuels) could be attributed to the increase in
heat  transfer  resulting  from  higher  gas  temperatures  and  the
increase of  compression work.   Gas temperature and compression
pressure increases  can be  explained based on the  thermodynamic
analysis of the pressure-volume equation of an ideal gas.

     6.  Emission results were obtained for both fuels, however,
definitive conclusions can not be drawn at this stage.

VIII. Future Efforts

     A 100 percent efficient methanol dissociator is currently not
available.  Presently, the best direction for this project may be
to evaluate what the  (2H2/CO)/CH3OH)  ratio is  for best emissions.
Running the engine on a mix of dissociated methanol and M100 may
yield more  power and decrease the uncontrollable  combustion and
flashback at high loads experienced with  2H2/CO operation.  Also,
an optimized mixture of vaporized and dissociated methanol may lead
to satisfactory cold  start  performance,  enhance  stability during
idling, and reduce exhaust emissions.

     Development and fabrication of a  dissociated methanol-assisted
injector adaptor is complete.  In this case, resistors can be added
to the adapters at a  small cost to enhance cold start operation if
it is needed.

-------
                              -21-
IX.    Acknowledgments

     The CA18DE engine  described in this report was modified for
use with M100 neat methanol and  loaned to EPA by the Nissan Motor
Corporation as support  for an effort to investigate the potential
of neat methanol as an  alternative motor vehicle fuel.

     The authors appreciate the  efforts of Marc Haubenstricker of
the Fuels and Chemical  Analysis  Branch for FTIR analysis support.
The authors also appreciate the  efforts of Jennifer Criss and Mae
Gillespie  of the  Technology  Development Group  for  typing  and
editing support.

X.   References

1.   "Hydrogen As A Fuel And The Feasibility Of A Hydrogen-Oxygen
Engine,"  Karim, G. and M.  Taylor,  SAE Paper 730089, January 1973.

2.   "State  of  the  Art  And  Future  Trend  Of  Hydrogen-Fueled
Engines," Furuham, S.,  JSAE Review, March 1981.

3.   "Ignitability Of Hydrogen-Air Mixture By Hot Surfaces And Hot
Gases In Hydrogen-Fueled Engines," Enomoto, K.  and S. Furuham, JSAE
Review, July 1981.

4.   "Hydrogen-Powered  Vehicle  With  Metal Hydride Storage  And
D.I.S. Engine System," Kama,  J.  and Y. Uchiyama, SAE Paper 880036,
February 1988.

5.   "Combustion  Characteristics  In  A  Hydrogen-Fueled  Rotary
Engine," Morimoto, K.,  et al., SAE Paper 920302, February 1992.

6.   "Conversion Of Methanol-Fueled 16-Valve, 4-Cylinder Engine To
Operation On Gaseous 2H2/CO Fuel-Interim Report III," Schaefer, R.
M., et al., EPA/AA/CTAB/91-01, April 1991.

7.   "Conversion Of Methanol-Fueled 16-Valve, 4-Cylinder Engine To
Operation On Gaseous 2H2/CO Fuel-Interim Report  II," Piotrowski, G.
K. and J. Martin, EPA/AA/CTAB/89-02, March 1989.

8.   "Resistively Heated Methanol Dissociater For Engine Cold Start
Assist-lnterim Report," Piotroski,  G. K., EPA/AA/CTAB/88-02, March
1988.

9.   Operation Manual For Engine Cycle Analysis Program, Power and
Energy International Inc., 1988.

10.  "Heat Release Analysis Of Engine Pressure Data," Gatowski, J.
A.,  et  al.,   SAE  Paper   841359,   Massachusetts   Institute  of
Technology, October 1984.

11.  "Factors Limiting  The Improvement In Thermal  Efficiency Of
S.I. Engine At Higher Compression  Ratio,"   Muranaka,  S.,  et al.,
SAE Paper 870548, February 1987.

-------
                               -22-


12.  "Basic Findings  Obtained From Measurement Of The Combustion
Process," Holenberg, G. and I. Killman, SAE Paper 820126, 1982.

13.  "Progress Report  On  In-House Dissociated Methanol Project,"
Note, from G.  K.  Piotrowski and R. M.  Schaefer to Charles L..Gray,
Jr., September 1991.

14.     "Study of the  Methanol-Reformed  Gas  Engine," Hirota, T.,
JSAE Review, March 1981.

15.   "Engine Operation on Partially Dissociated Methanol," Konig,
A., et al., SAE Paper  850523, February 1985.

-------
                               A-l
                            APPENDIX A
         TEST ENGINE SPECIFICATIONS, M100 FUEL OPERATION
               CONDITION AS LOANED BJLHISSJ
Manufacturer
Basic engine designator
Displacement
Cylinder arrangement
Valvetrain
Combustion chamber
Bore X Stroke
Compression ratio
Compression pressure
Fuel control system

EGR
Valve clearance
Idle speed
Engine oil

Fuel
Air/fuel control

Spark advance control
              Nissan Motor Co., LTD
                             CA18DE
                            1809 CC
                4-cylinder, in-line
             Dual-overhead camshaft
                    Pentrpof design
                    83 mm x 83.6 mm
                               10.5
  16.5 kg/square cm (350 rpm, 80°C)
          Electronically controlled
                     fuel injection
                       EGR not used
     0 mm (automatically adjusting)
                            750 rpm
    Special formulation supplied by
                Nissan for methanol
                   engine operation
                 Ml00 neat methanol
Excess air ratio may be varied from
             0.5 to 2.0 by means of
                an external control
      Ignition timing can be varied
    from OOBTDC to 54«BTDC by means
             of an external control

-------