EPA-AA-TEB-81-12
Evaporative and Exhaust Emissions of Two Automobiles
       Fueled  with  Volatility Adjusted Gasohol
                         by
                 David C. Lawrence

                 Daniel J. Niemczak
                   December  1980
             Test and Evaluation Branch
        Emission Control Technology Division
   Office of Mobile  Source Air  Pollution Control
       U. S. Environmental Protection Agency

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                                    -2-
Abstract

This paper presents the  objectives  and  results of a vehicle emission test
program conducted  by  the U.  S.  Environmental Protection  Agency  (EPA)  in
July, 1980.  The program was  designed  to investigate the effects  of using
various  gasohol blends  on  vehicle  evaporative  and  exhaust  emissions.
Particular emphasis  was directed  towards  a  blended gasohol  whose vola-
tility characteristics  (ASTM distillation  and Reid vapor  pressure)  were
adjusted  to  match  as  closely as possible  those of a  baseline gasoline.
Two vehicles received  triplicate tests on  each  of four fuels: 1)  a  com-
mercial  grade   unleaded  gasoline,  2)   a blended  gasohol   containing  10%
ethanol with volatility  characteristics  similar  to Fuel  1, 3) a mixture
of  10%  ethanol and 90%  Fuel 1,  and 4)  a  mixture of 5%  ethanol  and  95%
Fuel 1.   The analysis  also included a  gas  chromatograph characterization
of  the SHED  vapors for ethanol  concentrations and  a comparison of carbon
balance fuel  economy versus volumetric  fuel economy.

Results indicate  an overall  increase   in the  total evaporative  HC emis-
sions for  all  three  gasohol  fuels.   Blended  gasohol  exhibited the lowest
increase of 41% while  the  10% and 5% gasohol  mixtures showed increases  of
58% to 62%.  Exhaust HC, CO and  NOx  were reduced with  the  blended gasohol
and 10%  gasohol mixture when compared  to  the baseline  gasoline.   The  5%
gasohol mixture resulted in little   or  no change.  For  one  test  vehicle,
the volumetric  and carbon  balance fuel economy  showed  a decrease tor  all
three gasohol  fuels,  while  the  other  vehicle resulted in little or  no
change.    In  comparing  the  two methods  of  fuel  economy  measurements
(carbon balance and volumetric)  the volumetric  method was  consistently
0.6% higher.

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                                    -3-
Intreduction  '

As  the production  capabilities  of  ethyl  alcohol and  its  use  as  a fuel
additive  in the  form of  "gasohol" increase,  continued  research  of its
effect  on  vehicle emissions is warranted.  An  earlier  study conducted by
the  U.  S.  Environmental  Protection Agency  (1)* showed that  the largest
detrimental  effect  on emissions  caused  by the use of  gasohol. was  in the
area of evaporative hydrocarbon  (HC) losses.   This report  stated that an
average  increase  of  49  - 62% could be  expected using the  current auto-
mobile  fleet and  method  of gasohol  production.  Presently,  commercial
gasohol  is  produced  by  "mixing"  10%   (by  volume)  ethyl  alcohol  (or
ethanol) and  90%  finished commercial gasoline.   This addition  of ethanol
drastically  alters  the  volatility  of the fuel  which  results  in  higher
evaporative  emissions.   One  suggested  solution to  this  problem   is  to
"blend"  the gasohol  at  the  refinery using heavier base  stocks  to  end up
with  a  gasohol  with  volatility   characteristics  (ASTM distillation  and
Reid vapor  pressure)  similar  to  commercial gasoline.  As  a result of this
concept, a test program  was  designed to  investigate the  effects of such a
gasohol on evaporative and exhaust  emissions.

The  program  consisted  of  two  late model passenger  cars  that  received
triplicate  evaporative  tests using  a commercial  grade  unleaded gasoline,
a  special  blended  gasohol  with  modified  volatility  characteristics,  and
two mixed  gasohol  fuels  containing  5% and  10%  ethanol.   Secondary objec-
tives of the  test  program included  an evaluation of  exhaust  emissions,  a
comparison  of volumetric  and  carbon balance fuel economy  measurements and
gas chromatograph analysis of the  SHED vapors for ethanol content.

The  purpose of this  report is to present the  procedures,  equipment and
results of this investigation.

Test Procedure i

The  test  procedure  used  in  this  program consisted  mainly  of  the  1977
Federal  Test  Procedure (FTP) for  evaporative  and exhaust  emissions  (2).
Slight  deviations from this  procedure  were introduced to  accomodate addi-
tional  data  acquisition  and instrument  operation.  However,  these  proce-
dures  were  usually  introduced  at  times  during  the  FTP  which  allowed
completion  of the  task  while still following  the  FTP time  constraints.
The deviations;from the  FTP  are  listed belc; and a  complete test sequence
is given in Appendix A.

         The  vehicle  charcoal cannister  was weighed  before  and  after the
         Diurnal  Heat Build  and  the  Hot  Soak  evaporative  loss  tests.
         This was performed within  the  FTP time limits.

         A  volumetric  flowmeter   was  connected  in  series  between  the
         carburetor  and  the  fuel  pump.   An  electric   fuel  pump  was
         installed  on each vehicle  and  used to  prime  the  flowmeter  and
         float bowl prior to each driving cycle.
*Numbers in parentheses designate references at the end of the paper.

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                                    -4-
         A  gas  chromotograph  was  connected  thru  a  sample  port  to  the
         SHED.  A  vacuum pump  was used  to  inject  the SHED vapor into the
         column and  it  is  estimated that about  .5  liter  was  removed from
         the SHED per injection.

         Fuel  density  was  measured  immediately  prior  to each  driving
         cycle by means of an API hydrometer.

         Engine  parameters  such  as  the water  jacket,  engine  oil,  and
         carburetor  bowl temperatures  were recorded  during   the  driving
         cycle and Hot Soak  loss portions of the FTP.

The  original  test  plan called  for triplicate  tests to  be  run  by each
vehicle using each tuel.  However,  due  to  void  test make-up  and a short-
age of  test  fuel,  only duplicate tests  were  run by each  vehicle  on some
of the test fuels.

Test Fuels

The four fuels chosen for the program were tested in the following order:
              i
    Fuel 1:   !A commercial  grade  unleaded  gasoline  used   as  the baseline
              fuel.

    Fuel 2:   A blended  gasohol containing  10%  ethanol and  90% unleaded
              gasoline having  volatility characteristics   similar  to that
              of Fuel 1.

    Fuel 3:   A mixture  (by volume)  of 10% ethanol and 90% Fuel 1.

    Fuel 4:   A mixture  (by volumeJ  of 5% ethanol and 95% Fuel 1.

The  test   fuels  were selected  to  investigate   two  suggested methods  of
reducing evaporative  hydrocarbon  emissions  trom gasohol  fuelea vehicles.
The first method is  that of  blending  the gasohol to have   lower volatility
by using heavier base stocks and adding ethanol.   The secona  method  was
to reduce the concentration of the ethanol to 5%.

The volatility  match between  Fuel  1  and  Fuel  2  turned   out  to  be  very
difficult  to  obtain within the original specifications of identical Reid
vapor  pressure  (RVP) and  ASTM distillation  curves  within  +_5°F  of  each
other.   The  fuel  finally  purchased   from  the  Amoco  Oil   Company  in
Naperville, Illinois was within 0.1  psi RVP and +20°F ASTM distillation.

Fuel 3  is  a  mixture of  10%  ethanol and  90%  Fuel 1.   This  fuel represents
a typical gasohol currently on the commercial market.

Fuel 4  is  also  a  mixture with  5% ethanol  and  95% Fuel 1.  This fuel  was
used to investigate the effects of a lower concentration of ethanol.

The  fuel  characteristics for all four  fuels are  shown  in Table  1  ana  a
comparison of the  ASTM  distillation data is  displayed in  Figure  1.   The

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                                    -5-
test  fuels  were  stored  in  sealed  drums  until  testing  started on  that
particular  fuel.   They  were then  tranferred  to  a  vented,  chilled  fuel
cart and kept at 48 - 52°F.

The  fuels  were tested  in the  specified  numerical order except  that  the
baseline fuel  (Fuel  1) was  repeated  at the end  of  the test  sequence  to
confirm that the baseline results did not shift.
                                     Table  1
                              Fuel Inspection Data

               Fuel 1             Fuel 2           Fuel 3        Fuel 4
  ITEM      Baseline Gasoline   Blended Gasohol   10% Gasohol   5% Gasohol

1. API Gravity    54.9              49.2              54.2         54.6

2. Sp. Gravity    .759              .783              .762         .760

3. R.O.N.         95.2              99.4

4. M.O.N.         84.3              87.2

5. RVP, PSI       9.3               9.4               10.2         10.4

6. ASTM Dist.

     IBP          95°F              102°F             92°F         97°F
     10%          120               128               118          116
     20%      ;    143               147               133          129
     30%          173               160               146          146
     40%          208               194               156          186
     50%          240               258               210          226
     60%          267               278               251          257
     70%          294               301               281          286
     80%          320               321               311          314
     90%          354               350               345          348
     EP           432               434               425          424

Analysis
Performed:     Amoco Oil Co.     Amoco Oil Co.     Ethyl Corp.    Ethyl Corp.
by

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                                       -6-
450
                                     average carb. bowl temperature
                                     for all fuels
                                           Fuel 1: Baseline Gasoline  (RVP=9.3.)
                                           Fuel 2: "Blended Gasohol"  (9.4)
                                           Fuel 3: 10% ethanol & 90%  Fuel  1  (10.2)
                                           Fuel 4: 5% ethanol & 95% Fuel  1  (10.4)
              —r—
              20
—-i—
 30
—r
 40
—r-
50
—r—
 60
—i—
 70
—I—
 80
—r~
 90
100
                        Percent  Evaporated
           Fig.  1 - ASTM Distillations  for Test Fuels

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                                     -7-
Test Vehicles

The  two  test vehicles used  were a 1979  Buick  Regal and  a  1979 Chrysler
LeBaron.   Vehicle  specifications  for  these cars  can  be  found  in  Appen-
dix B.

Prior to  testing,  the vehicles were inspected  and adjusted  to meet manu-
facturer's specifications  and  the mechanical fuel pump  was  bypassed with
an electical pump.  This  pump  was necessary to  prime the volumetric flow-
meter and  float bowl prior to each test.

Instrumentation of  the vehicles  included  bare-bead,  type  J  tnermocouples
located  in the fuel  tank, carburetor  bowl,  engine oil pan,  and  in  the
engine water  jacket.   The  engine parameters were measured  as indicators
of  test  condition  and load repeatability and  the  fuel  parameters were
correlated back to the evaporative emission results.

Fuel  flow was  also measured volumetrically using a flowmeter  which  was
placed between the  fuel  pump and  the  carburetor.   The  same  flowmeter was
used  for  both  cars  and was  connected  and  primed  before each  test.   Fuel
density was also measured at this time using an API hydrometer.

Gas Chromatograph Analysis

The  gas  chromatograph analysis of  the SHED vapors  was  used  to quantita-
tively determine  the  concentration ot  ethanol  vapors in  the  evaporative
emissions.   The  gas  chromatograph (G.C.)  used  was a Perkin-Elmer  Model
3920  witn  dual FID detectors.   The  column consisted of  ten  feet  of  1/8
inch  O.D.  tubing  packed  with  tris  (cyano  ethoxy)  propane.   The  column
temperature was kept  at 50°C which resulted in the  ethanol  peaking  at 15
minutes.   A  sample  pump  (from  a  Philco Ford CVS) was used  to inject  the
vapor into the  column and the  G.C. response was  traced  on a  strip chart
recorder.  The peak widths were assumed to  be  relatively  constant  and no
effort was-made to integrate the peak areas.

The  G.C.  was calibrated  prior  to the program using  the  following  proce-
dure:  After stabilizing  the instrument at  the  indicated  temperature  and
purging  the  column  (for  three  days)  a small petri  dish  containing anhy-
drous ethanol  was  left  partially  uncovered on  a balance  in  the  SHED.
Immediately  after  the SHED  was  sealed,  an initial  sample  was  injected
into  the  G.C,  and the  digital  balance  reading  recorded.    Then,  at  a
frequency  determined  by  the G.C.  sampling rate,  additional  samples were
injected  and  weights   recorded  as  the ethanol  slowly evaporated.   This
procedure  was  repeated once and  the  data reduced to a  grams  ETOH  versus
G.C.  response  curve.   A  linear regression  revealed  a  linear  relationship
(coefficient of determination,  R^ =  .9939) and a SHED  volume correction
factor was introduced  to  account  for  a vehicle in the SHED.   However, no
corrections  were  made for  barome,tric  pressure  or  ambient  temperature
variat ions.

Test Results

EVAPORATIVE EMISSION  RESULTS -  The  evaporative HC emission  test  results

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                                    -8-
 for  each  vehicle are presented  in  Table  2.  The  average  results for  the
 program  are  presented in  Table  4  arid  displayed  graphically in Figure  2.
 These results demonstrate  several noticeable  trends.

 Considering  the  blended  gasohol  (Fuel 2)  first, the total vapor  generated
 (vehicle  canister  weight  gain plus ShED  evaporative  results)  using  this
 fuel  was  3%  less than the total vapor generated by the baseline  gasoline
 which would  be  expected  because  of the lower  front  end volatility of  the
 blended  fuel (see  Table 4).  However,  the  total  SHED test emissions  were
 41%  higher  than the  baseline  gasoline.   Breaking  this  down  into   the
 Diurnal  Breathing  Loss  (DEL) and the  Hot Soak Loss (HSL) portions of  the
 SHED  test,  shows  that  most  of  the  evaporative   emissions  increase  came
 from  the  HSL  test   where  a  21%  increase  in the  vapor  generated   was
 observed.  This  can  be  explained by examining the distillation curves  for
 both  these  fuels  and noting  that  the highest achieved  carburetor  bowl
 temperatures  during   the  HSL  tests were  above  150°F where  the blended
 gasohol  is more volatile  than  the  baseline fuel  (all  the  gasohol fuels
 had  carburetor  bowl  temperatures of about 153°F and the baseline  gasoline
 had a carburetor bowl temperature of about  156°F).

 The  total  vapor  generated during the  DEL test dropped by about  13%  when
 using blended  gasohol,  however  the evaporative losses rose  by 6%.    This
 indicates  an effect  on  the  trapping efficiency of  the canister  charcoal
 by the  alcohol.   This efficiency loss  was  1% (not statistically  signifi-
 cant) for  the  LeBaron and 4%  for  the  Regal.  It  is hard  to  determine  if
 the  alcohol  is  being  preferentially  absorbed  by the  charcoal  since   the
 gas   chromatograph   data   varied  widely   for  each  test  vehicle.     The
 LeBaron1s  ethanol  emissions accounted for 12% of the total  losses  when
 using blended  gasohol,  while the Regal"s  ethanol  loss accounted  for  only
 2%.  The gas chromatograph data  is  presented  in Appendix C.

 In comparing the 10% ethanol - 90%  baseline  fuel  mixture  (Fuel  3) to  the
 baseline  fuel,   a  24% increase  in  the total vapor  generated and  a   58%
 increase  in  the total   evaporative losses  can be  seen  (see  Table   4).
 Again, the increased volatility  of the mixture is the primary reason  for
 these increases, but compounding this  is  the trapping efficiency  decrease
 (about 3%  average) of the  charcoal  canister.  The fuel mixture containing
 5% ethanol and  95%  baseline gasoline  (Fuel  4)  exhibited  similar  evapora-
 tive  emission  results as  did  Fuel  3.  The  total  vapor generated rose  to
 25%  compared to the baseline   fuel  resu^-,  and  the  total  evaporative
 losses rose  62%.  This  fuel  had the highest Reid  vapor  pressure and  low
 end volatility which caused  the  Diurnal losses  to increase 106%.  The  Hot
 Soak  losses  rose  20%  which  was the  lowest  of  the  three  gasohol  fuels
 tested.

 EXHAUST EMISSION RESULTS  - The exhaust emission  results  for  each vehicle
 are  presented   in  Table  3.   The   average  results  for  the  program   are
 presented in Table 5 and displayed  graphically  in Figure 3.

 In comparing the blended gasohol and  the  10% gasohol mixture to the base-
 line  gasoline rwe find  a significant  decrease  in the exhaust  HC,  CO  and
 NOx emissions.    HC decreased by  8% for  the blended  gasohol  and 23%  for
 the  10%  gasohol mixture,  while  CO decreased  35% and 40%  respectively.
NOx emissions were  reduced 22% for  the  blended  gasohol and 3% for the  10%

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                                   -9-
gasohol mixture.  This can  be  explained by noting the  leaning  effect the
ethanol has on  the air/fuel  ratios.   NOx  emissions may have been affected
by  cylinder  temperature variations  due  to  the  presence  of  ethanol.
However,  for  the 5%  gasohol  mixture,  the  leaning  effect  is  not  as
apparent since  the exhaust emission results  closely  resemble  those of the
baseline fuel.

FUEL ECONOMY  RESULTS -  For  this test  program  tne  EPA city  fuel  economy
was measured  by both  the  carbon balance  method and  using a  volumetric
flowmeter.   However, due  to  a  lack of  availability of  the  flowtneter
Fuel 4  was  not  measured volumetrically.   The  average  results   for  the
program are  presented  in Table  5  and displayed graphically  in  Figure 3.
Figure 4  provides  a  comparison  of  the carbon  balance method versus  the
volumetric measurement.

For all the  gasohol  fuels  tested,  a  slight  decrease  in  the  average  fuel
economy was  observed for both  the carbon  balance  method  and  the  volu-
metric  measurement  when compared  to  the  baseline  gasoline  (one  vehicle
showed  a  decrease  while  the other  vehicle  showed  little or no  change).
The  10%  gasohol  mixture  produced  the  largest  decrease  of  2%.   These
results are expected since  the  energy content of gasohol is known to be
below that  of gasoline.   However, other  sources have  shown  that  ethanol
burns more  efficiently in the  combustion  chamber  thereby  minimizing  the
effect of a lower energy density.

In comparing  the volumetric  measurement to the  carbon balance method,  the
volumetric measurement was   consistently  0.6%  higher.  A summary of  the
calculations used for the carbon balance method is  given in Appendix P.

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                                      -10-
Table 2 - Evaporative HC Emission Results for Individual Vehicles

1979 LeBaron
                                             Vehicle Canister
                                             Weight Gains (gm)
SHED Results
Fuel N
Fuel 1 5
Fuel 2 3
Fuel 3 3
Fuel 4 2
1979 Regal
Fuel N
Fuel 1 5
Fuel 2 3
Fuel 3 3
Fuel 4 2
Notes: 1.
2.
3.
Diurnal Hot Soak
mean 1 .34
s.dev 0.25
mean 1.50
s.dev 0.04
% ch 11.9
me an 1.81
s.dev 0.09
% ch 35.1
mean 2.64
s.dev 0.66
% ch 97.0
SHED
Diurnal
mean 3.34
s.dev 0.79
mean 3.44
s.dev 0.65
% ch 3.0
mean 5.78
s.dev 0.80
% ch 73.1
me an 6.97
s.dev 1.33
% ch 108.7
HC results
% ch is re
To t a 1 v a po
2.46
0.20
3.67
0.35
49.2
3.36
0.17
36.6
3.33
0.40
35.4
(gm)
Total
3.80
0.16
5.17
0.36
36.1
5.17
0.08
36.1
5.97
0.27
57.1
Results (gm).
Hot Soak
2.45
0.74
4.95
0.35
102.0
4.17
0,14
70.2
2.60
0.04
6.1
Total
5.79
0.71
8.39
0.95
44.9
9.95
0.92
71.8
9.57
1.29
65.3
are not corrected
ferenced to Fuel 1
r generated = SHED
 Total Vapor
Generated (gm)
Diurnal
24.50
1.84
20.80
1.73
-15.1
25.03
1.69
2.2
30.20
0.99
23.3
Hot Soak
9.58
0.54
9.67
0.50
0.9
16.17
3.34
68.8
12.55
0,07
31.0
Vehicle Canister
Weight Gains (gm)
Diurnal
21.84
0.53
18.47
0.84
-15.4
22.43
0.96
2.7
21.85
2.05
0.04
Hot Soak
7.70
0.75
8.67
0.23
12.6
12.20
2.21
58.4
11.70
0.14
51.9
Diurnal Hot
25.84
1.62
22.30
1.71
-13.7
26.84
1.67
3.9
32.84
0.33
27.1
Soak Total
12.04
0.66
13.34
0.75
10.8
19.53
3.18
62.2
15.88
0.47
31.9
37.88
2.09
35.64
2.02
-5.9
46.37
4.08
22.4
48.72
0.79
28.6
Total Vapor
Generated (gm)
Diurnal Hot Soak
25.18
0.48
21.91
1.39
-13.0
28.21
0.24
12.0
28.82
0.72
14.5
10.15
0.38
13.62
0.54
34.2
16.37
0.18
61,3
14.30
0.18
40.9
Total
35.33
0.56
35.53
1.58
0.6
44.58
0.91
26.2
43.12
0.91
22.0

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                                   Til-
lable 3 - Exhaust Emissions and Fuel Economy Results for Individual Vehicles




1979 LeBaron


Fuel N
Fuel 1 4

Fuel 2 3


Fuel 3 3


Fuel 4 1

1979 Regal


Fuel
Fuel 1

Fuel 2


Fuel 3


Fuel 4

Notes: 1,
2.
3.
FTP Results (gm/mi)

HC CO NOx
mean 0.70 13.55 1.82
s.dev 0.02 0.58 0.12
mean 0.54 7.67 1.65
s.dev 0.05 0.86 0.29
% ch -22.9 -43.4 -9.3
mean 0.55 8.13 1.84
s.dev 0.03 0.23 0.02
% ch -21.4 . -40.0 1.1
mean 0.68 12.10 1.88
% ch -2.9 -10.7 3.3

FTP Results (gm/mi)

N HC CO NOx
4 mean 1.02 7.33 3.01
s.dev 0.16 0.71 0.13
3 mean 1.04 5.97 2.13
s.dev 0.06 0.67 0.51
% ch 2.0 -18.6 -29.2
3 mean 0.77 4.50 2.86
s.dev 0.02 0.10 0.11
% ch -24.5 -38.6 -5.0
1 mean 1.08 7.90 3.06
% ch 5.9 . 7.8 1.7
MPG
C.
C02 F.
533. 16
0.82 . 0.
535. 16
2.08 0.
0.4 1
- 523. 16
3.21 0.
-1.9 0
521. 16
-2.3 0



C02
469.
7.04
483.
2.65
3.0
472.
6.24
0.6
474.
1.1
HC results are not corrected for the ethanol
% ch is referenced to Fuel 1.
C.B.F.E. = Carbon Balance Fuel

Economy.
B.
E.
.4
05
.6
10
.2
.4
12
.0
.5
.6


C.B.
F.E.
18.9
0.24
18.4
0.06
-2.6
18.3
0.25
-3.2
18.3
-3.2
Vol.
F.E.
16.4
0.07
16.5
0.06
0.6
16.4
- 0.15
0.0
—
~ •

MPG
Vol.
F.E.
19.1
0.15
18.6
0.07
-2.6
18.5
0.10
-3.1
_
—
response of i




              Vol. F.E.  = Volumetric Fuel Economy.

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                                                 -12-
Table 4  -  Average Evaporative HC Emission Results for Test Program
                      Shed Results (gm)
 Vehicle  Canister
Weight Gains (gm)
Total Vapor
Generated (gm)
Fuel
Fuel 1
Fuel 2
Fuel 3
Fuel 4
Notes :
Table
Notes :
N Diurnal Hot Soak Total Diurnal Hot Soak Total Diurnal
10 mean 2.34 2.46 4.80 23.17 8.64 31.81 25.51
6 mean 2.47 4.31 6.78 19.63 9.17 28.80 22.10
%.ch. 5.6 75.2 41.3 -15.3 6.1 -9.5 -13.4
6 mean 3.80 3.77 7.57 23.73 14.18 37.91 27.53
% ch. 62.4 53.3 57.7 2.4 64.1 .' 19.2 7.9
4 mean 4.81 2.96 7.77 26.02 12.13 38.15 30.83
% ch. 105.6 20.3 61.9 12.3 40.4 19.9 20.9
1. HC results are not corrected for the ethanol response of the FID.
2. % ch is referenced to Fuel 1.
3. Total vapor generated = SHED results + vehicle canister weight gain
5 - Average Exhaust Emissions and Fuel Economy Results for Test Program
FTP Results (gm/mi) MPG
C.B. Vol.
Fuel N HC CO NOx C02 F.E. F.E.
Fuel 1 8 mean .86 10.44 2.41 501. 17.6 17.7
Fuel 2 6 mean .79 6.82 1.89 509. 17.4 17.5
% ch -8.1 -34.7 -21.6 1.6 -i.l -1.1
Fuel 3 6 mean .66 6.32 2.35 497. 17.3 17.4
% ch - 23.3 -39.5 -2.5 -.8 -1.7 -1.7
Fuel 4 2 mean .88 10.00 2.47 498. 17.4
% ch 2.3 -4.2 2.5 -.6 -1.1
1. HC results are not corrected for the ethanol response of the FID.
2. % ch is referenced to Fuel 1.
3. C.B. F.E. = Carbon Balance Fuel Economy.
Hot Soak Total
11.10 36.61
13.48 35.58
21.4 -2.8
17.95 45.48
61.7 24.2
15.09 45.92
35.9 25.4
               Vol.  F.E.  = Volumetric Fuel Economy.

-------
                                                           -13-
         SHED  RESULTS
  6.0 -i
  4.5 H
to
§3.0 -\
o
  1.5 H
        Diurnal
                          105.
                      62.4%

               ?.:.«*  •
                2     3
                 Fuels
                                             6.0 -
                                             4.5 -
S  3.0 H
M
O
                                              i.s  H
                                                   Hot Soak
                                                          75.;
                            20.3%
                                                           234
                                                             Fuels
                                                                                              Total
10.0 -j

 7.5 -

 5.0 -

 2.5 -

   0
                                                                57.7% 61-
                                                          41.3% pg;l
                                                                                                      Fuels
   40 -

   30 -

   20 -

   10 -
        VEHICLE CANISTER WEIGHT GAIN
        Diurnal
    0  J
                     2.4%
                           12.
                234
                 Fuels
                                                   Hot Soak


CO
s
M
u



20
15 -

10 -

5 -

n -

64 . 1%
:::::::$8

A 1 y :::-SH::::
,.:.H %m
SSSS: ::•::::&:
lil ilil
iiiiii li

S;5p |S^
          1234
                  Fuels
                                                                                              Total
                                                                                         60 -i .
                                                                                         45 H
                                                                                     c.
                                                                                         30 -|
                                                                                        15  H
                                                                                                   -9.5%
                                                                                                          19.2%  19
                                                                                                      2      3
                                                                                                      Fuels
   60  -

   45  -

|  30  -|
j
   15  H
        VAPOR GENERATED

        Diurnal
   0
                    7.9%
             -13.4%
                          20.9%
          1234
                 Fuels
   *  percent change from Fuel 1
                                             32 1
                                             24 -
                                                  Hot Soak
                                                               61.7%
          1     2     3
                 Fuels
 Fig. 2 - Evaporative HC  emission results (average of 2 vehicles)
                                                                                             Total
m
1
^t
e.
64 -
48 -
32 -
16 -
n —
24.2% 25.4%




-
•:•:-:•:.:•;.: ™»
-2-8Z III I
•:•:•:•:?::• SS?:$ xjj
111 11 1
HI ||

1 	 '•'•'•'•'•'•'• — -is*:-:1:-: ffifij
^
1
i
1
1
1
^L
                                                                                                    23
                                                                                                     Fuels

-------
                                         -14-
  2.0 -!

  1.5

  1.0

   .5 -
           HC
             -8.1%
                         2.3%
                  -23.3%
                2      3
                Fuels
           NO,,
 5.0 -,

3.75 -

2.50 -

1.25 -
    0
      -2.5%
-^1.6%|||f
       llli
                          2.5%
          1234
                Fuels
 * percent change  from Fuel 1
                                                   20 -I
                                                   15 -
                                                  10 -
                                                    5 -
                                                           CO
                                                                         -4.2%
                                                            -34.7% -39.5%i
                                                               2     3
                                                                Fuels
                                                          F.E.
                                                   19 -i
                                                   18 -
                                                   17 H
                                                   16 -
                                                   15
                                                               234
                                                                Fuels
Fig. 3 - FTP exhaust emissions and fuel economy results  (average of  2 vehicles)
                        20-1
                        19-
                                                    j	| Carbon Balance Fuel Economy
                                                        Volumetric Fuel Economy
17 -
16 -


Y//////S


'///////A


|

1 2 3
Fuels
                        *  percent change from carbon balance method

                        Fig.  4  -  Carbon balance versus volumetric fuel economy

-------
                                    -15-
Conclusions

Based  on  the  findings  of  this  test  program  several conclusions  can  be
made  concerning  the  emissions  effect  of "blended"  gasohol  and  "mixed"
gasohol fuels:

       1)   Blended  gasohol  exhibited approximately  41%  greater evapora-
            tive HC emission losses than the base fuel.

       2)   The presence of ethyl  alcohol  caused  about a  1-3% loss in the
            trapping efficiency of the canister.

       3)   Reducing the concentration of  ethanol  from 10%  t.o 5% does not
            reduce evaporative HC  emissions.  The  two mixed gasohol fuels
            (10% gasohol mixture  and  5%  gasohol mixture)  increased evapo-
            rative HC emissions by an average of 60%.

       4)   The blended  gasohol  decreased  exhaust  HC by  8% and  the  10%
            gasohol mixture decreased  exhaust  HC by  23%.   The  5%  gasohol
            mixture increased exhaust HC by 2%.

       5)   Exhaust CO decreased  4-40% with all the gasohol fuels.

       6)   NOx emissions  decreased  22%  with  the blended  gasohol  and  3%
            with  the 10%  gasohol mixture.   NOx  emissions  increased  3%
            with the 5% gasohol mixture.

       7)   Fuel economy (by carbon balance  and volumetrically) decreased
            about  1-2%  with  all   the  gasohol   fuels.   (One  test  vehicle
            showed a decrease while the  other  vehicle showed little or  no
            change).

       8)   The volumetric  fuel  economy measurement  was 0.6% higher  than
            the carbon balance method.
References

1.  Richard Lawrence,  "Gasohol  Test Program," EPA  Report  79-4,  December,
    1978.

2.  Federal Register, Vol.  41, No. 164, August 23, 1976

3.  California Air  Resources Board,  "Testing of  Three Caltrans  Gasohol
    Fueled Vehicles," Project 2F80E2,  May, 1980.

-------
     -16-
  Appendix A




Test Procedure

-------
                                   -17-
                           Gasohol Test Sequence

1.  Drain and refuel to 20% tank capacity
2.  Run 1 LA-4 driving cycle
3.  Hot soak one hour
4.  Drain and refuel to 40% tank capacity
5.  Run 1 LA-4 driving cycle
6.  Soak 12 - 24 hours at 68 - 75°F ambient temperature
7.  Run 1 FTP with SHED:

    a.   Diurnal Heat Build:

         - drain and refuel to 40% tank capacity (leave fuel cap off)
         - move vehicle to SHED
         - weigh vehicle canister and check canister lines
         - move vehicle into SHED
         - at 58°F fuel temperature, install fuel cap and  seal  enclosure
           doors
         - take gas chromatograph sample (at 60°F)
         - perform one hour diurnal heat build (at 60°F)
         - take gas chromatograph sample (at 84°F)
         - immediately weigh vehicle canister and check canister lines

    b.   Run 3-bag FTP emissions test within  60  minutes of  end of diurnal
         test

    c.   Hot Soak:

         - immediately after 3-bag emissions test, move vehicle to SEED
         - weigh vehicle canister and check canister lines
         - move vehicle into SHED and seal enclosure doors
         - take gas chromatograph sample and perform one hour soak test
         - after one hour, take gas chromatograph sample
         - immediately weigh vehicle canister and check canister lines

8.  Precondition for the next test

    a.   If using the same fuel,  go to step 5
    b.   If switching fuels, go to step 1

-------
            -18-
        Appendix  B




Test Vehicle Specifications

-------
OYNO SJTE:D005  TEST » 80-4176
                                                                                            PROCESSED* .09J49130  JUL  8t
     MANUFACTURER
                              VEHICLE SPECIFICATION REPORT  -(LO TESTING)-  DATE OF ENTRY t  6/35/80
                                               VEHICLE SPECIFICATIONS


                   VEHICLE ID  / VER  REPRESENTED CAHLINE  MODEL CODE
                                                                      DRIVE CODE
                                                                                      SOURCE
CHRYSLER
                        VMX-253
                                                           SEDAN
                                                                REAR DRIVE STR. LEFT
                                                                                                OTHER
                                                  DRIVE AXL WTS                     EOUIV.
VEHICLE                          MODEL.  ACTIVE   FULL    EMPTY    CURB    INRTIA    TEST    0/D    ACTUAL
 TYPE     ACTUAL VEHICLE MODEL   YEAR     YEAR    TANK     TANK   WEIGHT   CLASS    WEIGHT   CODE   DYNO HP
                                                                                                       RUNNING CHG
                                                                                                         NUMBER
NON-CER   LEBARON
                            79
                             79
                                                    4000P    4000P            11.9

                                                                         TIRE - SPECIFICATIONS
PRIMARY DURABILITY VEHICLE ID Ok ASSIGNED OF
                                            ALT. MANUFACTURER
                                                                        TIRE Si RIM
                                                                          SIZES
                                                                                              MFR
                                                                                            SWL BLT  PSI
                                                                                     CONSTR N M N M FT RR
                                                      ENGINE SPECIFICATIONS
DISPLACEMENT BORE
318. E

IGNITION
TIMING 1
•

IGNITION
TIMING 2
RATED
STROKE HP


TIM.
TOL.
•

TIMING
HPM
ENGINE
TYPE
ENGINE NO. NO.
CONFIGURATION CYL. CARBS
OTTO SPARK V-BLOCK

RPM
TQL.

TIM.
GEAR

f. CO
LEFT

% CO
RIGHT

* CO
COMH.
H

CO
TOL.
1

IDLE
RPM
TOTAL
# BBLS
?

IDLE
TOL.
FUEL SYSTEM FUEL COMP. COAST-
MFR/MOOEL INJCT? TURBO? RATIO DOWN TM


IDLE
GEAR
NO NO .
1
VO
ENGINE FAMILY ENGINE CODE '
  168
AXLE
RATIO
 N/V
RATIO
ODOMETER
                     730
   A/C
INSTALLED
                                           DRIVE TRAIN ANO CONTROL SYSTEM SPECIFICATIONS
EXHAUST TYPE
CRANKCASE
  SYSTEM
     TRANSMISSION
CONFIGURATION  CODE
EVAPORATION
  SYSTEM
FUEL TYPE
     MAIN-TANK
CAPACITY    VOLUME
                    YES     SINGLE RIGHT REAR   CLOSED        A-3


                                                   SHIFT SPEED
                AUX.-TANK
           CAPACITY    VOLUME
                                                                  CANISTER

                                                           EVAPORATIVE EMISSION
                                                             FAMILY        CODE
                                                                  UNLEADED (AT EPA-IND HO)


                                                                             SALES CLASS
   18. G
       7.2G
    EXHAUST RECYCLE
                      OXIDATION CATALYST
                                        CONTROL SYSTEM TYPES

                                        OTHER


                                    VEHICLE SPECIFICATION COMMENTS
                                                   7344  0
                                                                                         DYNO SITE»D005   TEST » 80-4178

-------
OYNO SITEtDOOS  TEST * 80-^224
                                                                                                   PROCESSED*
                                                                                                          JUL  8t  1980
     MANUFACTURER
                              VEHICLE SPECIFICATION REPORT   -
-------
           -21-
        Appendix C




Gas Chromatograph Raw Data

-------
                                          -22-
                     Gas Chromatograph Raw Data of Ethanol Vapors
Vehicle
BDB
ADB
BHS
AHS
DDE
DHS   Total
Test
Regal Blended #1
Blended #2
Blended #3
Mean
S.D.
10% #1
10% #2
10% #3
Mean
S.D.
5% #1
LeBaron Blended #1
Blended #2
Blended #3
Mean
S.D.
10% #1
10% #2
10% #3
Mean
S.D.
5% #1
def. gms.
2.2 .055
2.0 .050

4.5 .120
0.1 0.0
0.6 .010

0.2 0.0
1.6 0.38
2.0 .050

0.7 .013
0.2 .0
0.3 .002

0.6 0.10
def. gms.
7.8 .213
4.0 .106

5.8 .157
1.9 .047
2.0 .050

1.3 .030
16.8 .466
10.7 .295

12.0 .331
1.4 .033
2.2 .055

1.8 .044
def. gms.
5.8 .157
2.8 .072

3.7 .097
0.1 0.0
0.1 0.0

0.0 0.0
0.2 0.0
3.4 .089
5.4 .145

8.7 .221
0.0 0.0
0.1 0.0

0.0 0.0
def. gms.
9.1 .249
5.6 .151

6.1 .165
0.9 .019
5.0 .134

1.9 .047
4.2 .111
15.1 .418
13.7 .379

14.1 .390
4.1 .109
4.9 .131

4.9 .131
gms. gras. Test
.158 .092 .250
.056 .079 .135
.107 .086 .193
.072 .009 .081
.037 .068 1.05
.047 .019 .066
.040 .040 .080
.041 .042 .084
.005 - .020
.030 .047 .077
.111
.428 .329 .757
.245 .234 .479
.337 .225 .618
.109 .197
.318 .169 .487
.033 .109 -14z
.053 .131 .184
.135 .136 .271
.030
.034 .131 .165
Notes:   1.   BDB = before  diurnal  test
            ADB = after diurnal test
            BHS = before  hot  soak test
            AHS = after hot soak  test
            DDB = A  diurnal  test  (ADB - BDB)
            DHS = £  hot soak (AHS - BHS)

-------
                  -23-
               Appendix D




Carbon Balance Fuel Economy Calculations

-------
                                     -24-
                  Carbon Balance Fuel Economy Calculations

The  carbon balance  formula is  used to  calculate  the  fuel  economy of  a
vehicle  from  the exhaust  emission  data  gathered during the 1975  Federal
Test Procedure.  This equation  is in the  following  general  form:

              MPG = grams  of carbon/gallon of  fuel
                    grams  of carbon  in  exhaust/mile
From  this  general  Lui.uiua.ci, uuc C4ua
of a vehicle using indolene fuel  is:
                   formula,  the equation  for  calculating  the fuel economy
                   indolene fuel is:
              MPG =
                                 0.866 (.2798)
                    0.866[EHC] +  .429[ECO]
              where: 2798 = density of  indolene  fuel  (g/gal)
                        E = exhaust emissions  ( g/j&i )
                        .866,  .429  and  .273  are the  carbon  weight  frac-
                        tion of HC, CO  and CC>2 respectively

Since the  fuel  properties  of  the  baseline gasoline and gasohoi  fuels  used
in  this  test program  differ   from  indolene,  the  carbon  balance equation
had to be  modified  to  compensate  for  these differences.  As a result,  the
carbon balance  formula was reduced to the  following  form:
              MPG =
                                 D(W)
                     F[EHC] +  .429[ECO] +  .273[EC02]
              where: D =•  fuel density  (g/gal)
                     V/ =  carbon weight  fraction of  fuel
                     F =  carbon weight  fraction of  exhaust HC
                     E =  exhaust emissions  ( S'™1.)
The values of  D,  W and F
tabulated below:
                  D
                           for the  four  fuels tested  in  this program  are
                            W
D(W)
Fuel 1
Fuel 2
Fuel 3
Fuel 4
2867.12
2957.78
2878.45
2870.90
0.8702
0.8400
0.8341
0.8527
                                      0.8702
                                      0.8764
                                      0.8702
                                      0.8702
                                                2494,97
                                                2484.54
                                                2400.92
                                                2448.02
The  following  section  provides  a  brief  summary  of  the  equations  or
methods  used in  determining  the  above  values of  D, W,  and F  for the
various  fuels.   It should be  noted  that  the  carbon  weight  fractions of
the base gasoline  (Fuel  1)  and the blended gasohoi  (Fuel 2)  were supplied
by Amoco Oil  Company.  As a  result,  the  equation  to determine the carbon
weight  fraction  of the  fuel  was only applied to  the  10% and 5% mixtures
of gasohoi (Fuel 3 and Fuel 4).  These equations are as follows:

-------
                               -25-
     A.   Calculation of fuel density:

          fuel  density =  specific  gravity  A2_J  X  density  of  water
          at 60°F                            60°

     B.   Calculation of carbon weight fraction of the fuel (3):

          Carbon weight fraction = A(W) D  + B(K) £
where:    A = volume percent of gasoline used in fuel mixture
          W = carbon weight fraction of gasoline used in fuel mixture
          Dg = density of gasoline used in fuel mixture (g/gal)
          Df = density of gasohol fuel (g/gal)
          B = volume percent of ethanol used in fuel mixture
          K = carbon weight fraction of ethanol used in fuel mixture
              = .5214
          De = density of ethanol used in fuel mixture = 2979.18
              (g/gal)

     C.   Calculation of carbon weight fraction of exhaust  HC :
          1)     This  calculation   involves   no  equations   only   2
                 assumptions.

                 a) For  gasoline,  the carbon  weight fraction  of  the
                    exhaust HC is the  same as  the  carbon weight frac-
                    tion of the fuel.

                 b) For gasohol, the  fraction of ethanol contained  in
                    the  exhaust  is  minimal  (it is  less  than  .1%  of
                    the  measured exhaust  hydrocarbons  (3)).    Thus,
                    the carbon  weight fraction of the  exhaust  HC  for
                .'  '  gasohol will  be  the same  as   the  carbon  weight
                    fraction  for  the gasoline  used  in the  fuel mix-
                    ture.

-------
          -26-
      Appendix E




Individual Test Results

-------
                            Individual Test  Data
                                1979
Fuel Test Date
R>E£.l
Fuet£
FOa.3
FUEL 4-
FuEiJ.
/i
£
3
.1
a
3
A
£
3
J.
a

j.
2.

^2/80
t/25/ao
6/26/80
7/6/^0
7/7/50
7/"?/(9o
T//5/09
7A7/90
r//?/9c
rfeo/eo
7/22/eo

7 /&/80
7/24/&0

FTP (gm/mi)
HC CO NOX CO 2
.7^
.69
.72.
.48
.3-8
.55
.52
.58
.55
.68
—

,68
—
	
/3.7
/2.8
/f.2
7.5"
6.?
a 6
ao
8.4
8.0
12.1
—

/3.^



/.76
A 68
A87
A 33
/-87
/.76
1.85
1,85
I.&2.
1.88
—

135



53^
53Z-
533.
533-
531.
537.
524.
5fr
5^5
52/-
—

53$.
	

mpg
C.B. Vol.
16,4
\6.S
\t>A
/6.7
/ 6. 6
\(oS
16.3
\b5
J&3
16.5
—

/6.4
—

/6.4
/6^5
—
I6,5~
/6.5
16,4
16.4-
|6.6
/6.3
—
— -

—



SHED (gm)
DEL HS Total
1.78
I./9
l.lt
l,5/
/.53
1^5
1.82.
1.72.
I.Jo
2.17
3.11

1.22
/.Iff

ZJ5
a..^
2.^3
3.30
4-. oo
3.71
3AI
3.5-0
3- /6
3.61
3,05"

2.5"?
£.5-7

3.93
355-
3.9*
4.8/
5:53
51/6
3T23
5:.2a
3:08
5:78
6./6

379
3.75"

Can. Wt. (gm)
DEL HS
ai-4-
24.3
£5:a
183
21. ^
£2.3
23./
26, a
25". 8
3a ?
2?. 5"

26.0
25: £

9.3
9,3
/a a
96
10.2
?.2.
14.6
13.9
2o.b
/2.6
/££"

/a/
9,o

Tot. Vap. (gm)
DEL HS Total
23.18
25:49
26. 5"/
£0.41
22.73
23.75'
24.72
27.92
27.70
33,07
32.61

27.21
24.7£

//.45~
\\.bto
£.83
(2.9o
14.20
I2.^/
/ao/
/?.4o
2a/a
/6.2/
&&>'

/2.67
//o'?

34.^3
37./3"
3^3f
33. 3 /
36. ?3
36. ^6
42. -?3
457 3£
50. BB
4?. 28
4^./6

3^.89
3535'

Key:  C.B.= FTP Carbon Balance Fuel Economy
      Vol.= Volumetric Fuel Economy
      DBL = Diurnal Breathing Loss
       HS = Hot Soak
 Can. Wt. = Canister Weight Gain
Tot. Vap. = Total Vapor Generated

-------
Individual Test Data
    1979  RE6-/U.
Fuel Test Date
FuELl
Fl'GL *2
F^'Et- 3
FUE*. 4
F^l
1
e
3
1
a
3
J.
2.
3
.1
a

i
/a

6/a;/Bo
6/30/ao
7/2/80
r/b/so
7/7/80
7/7/60
7//5/8C'
7/17/80
7//8/80
r/2i/ao
7/22/80

*7 1^180
7/£4/#0

FTP (gm/mi)
HC CO NOV CO 2
/.GO
,9/
'?/
i
£.(*$
£86
3.32
4, /4
6.55
^6>3
4.96
7.9/
6,e>3

4-40
3.3o

^.^
3.00
3,03
4.^
4.^
57^3
4>24-
4,27
4,o/
2^7
2.63

/.7*
I.S4-

5o
5.71
271 .
7.18
9.47
70.79
10.10
897
10 AS
& 66

6./4
4.6'f

Can. Wt. (gm)
DBL HS
an
^2.$
^^~l
/7.5"
/f.o •
td.1
&\.+
az.
-------