EPA-AA-TEB-511-80-7
       EPA Evaluation of the Basko MW Enginecoat Under Section 511
          of the Motor Vehicle Information and Cost Savings Act
This document  contains  several pages which  may not reproduce  well.   Any
questions concerning the legibility of  these  pages  should  he directed to:
Merrill  W.   Korth,   Environmental  Protection  Agency,  Office  of  Mobile
Source Air Pollution Control,  Emission  Control Technology  Division,  2565
Plymouth Road, Ann Arbor, MI  48105,  (313) 668-4299 or FTS 374-8299.
                                   by


                          Edward Anthony Earth
                       Test and Evaluation Branch
                   Emission Control Technology Division
              Office of Mobile Source Air Pollution Control
                   TT.S. Environmental Protection A^oncy

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EPA  Evaluation  bE  the "Basko  M-W  Enginecoat"  Under  Section  511 of  the
Motor Vehicle Information and Cost Savings Act

The  following  is  a summary  of  the information on the Device  as  supplied
by the Applicant and the resulting EPA analysis and conclusions.

1.  Marketing Identification of the Device:

    Basko MW Enginecoat

2.  Identification of Inventor and Patent:

    Inventor

    William J. Manning
    220 Forest Ave.
    Wyoming, OH  45215

    Patent
    Pending

3.  Manufacturer of the Device:

    Bolce Paint Company
    4011 Red Bank Road
    Cincinnati, OH  45227

4.  Manufacturing Organization Principals:

    Earl Bolce
    Val Jacobs

5.  Market ing Organization/Applicant:

    Bask Industries, Inc.
    P.O. Box 15113
    Cincinnati, OH  45215

6.  Applying Organization Principals:

    William J. Henning  (contact)
    Ann S. Henning

7.  Description  of Device:	Purpose,  Theory,  Detailed  Description (as
    supplied by Applicant;

    A.   Purpose:   "Improved  engine performance and  increased tuel econ-
         omy ."             .

    B.   Theory  of Operation:   "There are two coatings,  one to dissipate
         and  one to  insulate.   Coating  is  applied  like  a  paint  to the
         exterior  surface of  the  intake manifold  giving,  faster heat and a
         hotter  interior  intake manifold  surface.  This  results in better

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         vaporization  of  the  gasoline giving  increased performance  and
         better fuel  economy.   The other  coating  dissipates  heat and  is
         applied to the exhaust manifold and engine block."

    C.    Description:  "Paintlike coating."

8.   Applicability of the Device (as supplied by Applicant):

    "All gasoline and diesel internal combustion engines."

9.   Device  Installatioii  -  Tools  and  Expertise  Required, (as supplied  by
    Applicant:

    "Easily applied with a paint brush."

10. Device Operation (as supplied by Applicant):

    "Not Applicable."

11. Device Maintenance (as supplied by Applicant):

    "Not Applicable"

12. Effects, on  Vehicle Emissions  (non-regulated)  (as supplied  by  Appli-
    cant):

    No information supplied.

13. Effects on Vehicle Safety  (as supplied by Applicant):

    "None known"

14. Test  Results  (Regulated  Emissions and  Fuel  Economy (as supplied  by
    Applicant):

    "Lowers HC  and  CO.  NOx not known.   In  addition to  actual  tests done
    on  vehicles' we  had  some  dynamometer tests  conducted.  These  tests
    substantiated our  actual  tests and provided information regarding the
    lowering  of HC  and  CO.   I  am enclosing copies  of  two  letters,  one
    from  a  taxi cab company,  and  one  from a trucking company.   The fleet
    average miles for  gallon  of gasoline for the  cab  company is 10.  The
    average for the trucking  company  is  5.04 miles  per  gallon  of  diesel
    fuel.   I  might  add  that  we  only  coated  the  intake manifold .on  the
    trucks  and  cabs'.  The  addition  o.f the  dissipating  coating  is  a more
    recent development.  Hopefully this v/ill lower iJOx."

16. Analysis

    A.    Marketing Identification of the Device:

          The  Device  (product)  is identified  in  Section  1 as   "Basko  MW
          Enginecoat."   However,  in  Section  7  the  applicant  describes
          "  .  .  two  coatings,  one  to   dissipate   am!  one  to  insulate."
          There  are  therefore  clearly two  Devices   (product-r.)  described

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       with  opposite properties.   The  Applicant is  therefore  judged to
       have  not  clearly  described the  marketing identification  of the
       Devices  (products).

    B.  Identification of  Inventor  and Patent

       As  an enclosure  to a letter dated January 20, 1981 (Attachment A)
       the Applicant  provided  a   copy  of  the  recently  issued  patent
       No. 4,240,936 (Attachment B), covering the insulative coating.

       The Applicant did  not provide  a  patent description of the conduc-
       tive  coating.

    C.  Description  of the  Device:

       (1)  The Applicant's stated purpose  of  the Device,  as  stated in
       Section  7A,  is  "Improved  engine  performance and  increased  fuel
       economy."   However the  theory  of operation as  stated  in Section
       7B  and Attachment  A are  conflicting.

             In Section 7B  the  Applicant  stated  the "coating  is applied
             like a paint to the exterior surface of the intake manifold
             giving faster  heat  and  a  hotter  interior  intake manifold
             surface.   This  results in better  vaporization  of  the  gaso-
             line giving  increased performance  and better fuel economy."

             In Attachment A the  Applicant stated  "In  other words,  when
             the  coating   is applied  to the exterior surface  of  the in-
             take manifold, we are  in  effect creating  a  cooler  fuel
             charge which  gives  better engine  performance  and  better
             fuel economy."^'

             The  Applicant  has therefore  claimed   the  Device (product)-
             gives  better performance  and fuel  economy by simultaneously
             both heating and  cooling the  fuel-air charge.

        (2)  The Applicant states  in  Attachment A  that  ".   .  .  you  will
       note  that  the  coating  when applied  away  from a heat  source in
       thin  coats   has   the  capability   to  release   heat  faster   than
       normal.  . This assumes that the high eciissivity coating is applied
       to  a low  emissivity  surface.    Such  could be  the case  with the
       intake  manifold."  Although this  is  true in  theory as acknowl-
       edged by EPA in the  note (I)  on page 3,  this  effect is unlikely
       to   occur   in   practice  since   intake   manifolds  arc  normally
       painted.  The painted surfaces emissivity would  typically be
         The  Applicant  is  correct  in  stating in  Attachment A  that  an
insulating product applied-in  thin  coats  will  increase the heat  transfer
in some cases.  This  occurs  when a high emissivity insulation is applied
in a  sufficiently  thin layer  to  a  low emissivity  surface.   This  occurs
because  the   increase  in  radiant  energy  for  the  insulated  surface  is
greater than the decrease in  conductive  energy.

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         between  .85  and  .95,  nearly  the  same  as  the  Basko coating's
         eniissivity of  .94.   It  is  also  unlikely a  manufacturer would
         select  this  product  for its  heat  transfer  properties  when a
         paint  presently  used would  have  very  similar  properties plus
         serve as a protective coating.

         (3)  Vehicle manufacturers  seek  to maintain  a  stable induction
         air  temperature  (typically  100°F) by  blending  warm  air drawn
         over  the  exhaust  manifolds  with  fresh  air.   This  permits more
         precise fuel-air calibrations to improve both emissions and fuel
         economy.   If   the  applicant's  device  did change   the  fuel-air
         charge  temperature,  the  net  effect would be  to  shift the fuel-
         air  induction  system's  calibration  from   the  manufacturer's
         design point to an off design point.

         (4)  The  second  product  described in Section  7B  is designed  to
         dissipate heat and is  to be  applied to the exhaust manifold  and
         engine block.

              (a)  The  Applicant  submitted  no information on or descrip-
              tion of this product.   EPA  is therefore  unable to judge  if
              this heat dissipation coating  is  able to  function.

              (b)  If  this  product were able  to  dissipate  heat,   its  use
              would not necessarily  be  desirable.   Lowered  exhaust mani-
              fold  temperatures   would  lower  exhaust   gas   temperatures.
              This could  adversely delay  catalyst "light off"  and also
              lower  catalyst   efficiency   under  many   vehicle  operating
              conditions.

    D.  Applicability of the Device:

         Since  the device  is  a  paint-like  product,  it  is able to  be
         applied to all gasoline  and diesel engines as claimed.  Informa-
         tion supplied  in  the patent  indicates the device (product) will
        "adhere to metal surfaces subjected to thermal stress.  Also,  the
         two  testimonal  letters  (Attachments  C-l,  C-2) supplied  by  the
         Applicant,  indirectly  infer the  product  is  durable  in  vehicle
         usage  application  (i.e.  no  complaints about  durability noted  in
         these letters).

E.  Device Installation - Tools and Expertise  Required:

    The Applicants  statement  that the  Device is  "Easily  applied  with  a
    paint brush" is misleading.

         (1)   The  patent  describes  a  Device with a  wide  range  in  the
         ratio  of  "pigment" to carrier vehicle and many different  carrier
         vehicles.  Not all of these  can be  expected to be applied  easily..

         (2)   Proper  application  of  the  Device  to  an  installed  engine
         would  be  difficult  due  to the numerous  hoses,  belts, liaes  and
         accessory equipment blocking ready  access.

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         (3)  Proper application of  the  Device to the total  exposed  out-
         side surface  of  either the intake manifold  or  exhaust  manifold
         would require removal of these manifolds  on most vehicles.

         (4)  An  important  part of  the  application  of  any  paint-like
         product to  a  surface is initial surface preparation  and surface
         preparation between  coats.   Proper surface  preparation is  many
         times considerably more work  than the actual application  of  the
         product.    The applicant  submitted no  detailed  information  on
         applying  the product.

F.  Device Operation:

    It is judged to be not applicable as  claimed.

G.  Device Maintenance:

    The  Applicant  states  none  is  required.  EPA is  unable  to  satisfac-
    torily  judge  this  statement  since   the  Applicant  submitted  little
    information by  which  EPA could  judge  the  long  term durability of  the
    product in automotive  use,  i.e.  its adherence to  the  surface  for  an
    extended time interval.

H.  Effects on Vehicle Emissions (non-regulated):

    The  Applicant   made  no  claims   nor  submitted any  data  relating  to
    unregulated emissions.  However, (a) since the Device  does  not  modify
    the  vehicle's emission  control  system and (b) any change  in inlet air
    or exhaust temperature could be  expected to be minimal,  the Device is
    judged to be unlikely to effect non-regulated emissions.

I.  Effects on Vehicle Safety and Operation:

    The  Applicant  claims   there  are  no known  adverse  effects  on vehicle
    safety.  This statement is judged to be probably  true.

    However,  the  actual  application of  the  Device  to  the  engine (i.e.
    painting)  may   entail  safety   hazards.   Most   paint-like  products
   . contain safety  warnings  that relate  to the components  of the vehicle
    and  pigment.  In extreme  cases  even special respiratory  equipment  or
    protective  clothing  is required.   Since  the Applicant  submitted  no
    information on  application safety and  many  paint-like  products  have
    safety  hazards, EPA  is  unable  to  conclude  that  application  of  the
    product is safe.

J•  Test Results (Regulated Emissions and Fuel  Economy):

    Applicant did not  submit  any test  data  per the Federal Test Procedure
    or Highway Fuel  Economy Test.  These  are the  only  EPA  recognized test

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proceduresv2)^   This  requirement   for   test   data   following  these
procedures is stated in  the Application  Format  EPA.  sends  to potential
applicants.   The  Applicant was  advised  of  this  requirement  on  five
separate occasions.

The test  data  submitted  by the Applicant are listed  below  and evalu-
ated.

     (1)  In  Section  14  the  Applicant  referenced  testing  done  on
          vehicles  and  some  dynamometer  testing.   However,  neither
          the  test vehicles nor  the  test  procedures were  described
          and  no   test results  were  provided.   Therefore  the  Appli-
          cant's  claim  of  lower 11C  and CO  emissions is  unsubstan-
          tiated.

     (2)  Two  testimonial  letters,  Attachments  C-l  and   C-2  were
          submitted  with  the  application.   The  writers  undoubtedly
          felt  they had achieved significant  fuel  economy  improve-
          ments with  the Bask products.  However,  even one  of these
          testimonials (C-l)  recognizes  that  it is  difficult to  be
          sure  that the  fuel  economy  change  was  due  to  the  Bask
          product.   Therefore,  because these were  uncontrolled tests
          of  the   Device,  they  cannot be used  to  evaluate  the  Bask
          device.

     On the basis  of information  supplied by  the Applicant, there was
     no need for the EPA to conduct confirmatory testing.

     Therefore, there  is  no  technical  basis  to  support  the  Appli-
     cant's claims  for fuel economy  improvement  for  "Basko  MW Engine-
     coat".                                                      ......
     From EPA 511 Application Format:
     Test Results (Regulated Emissions and Fuel Economy):
     Provide  all  test information  which  is available on  the effects
     of the device on vehicle emissions and fuel economy.

     The  Federal  Test Procedure  (40  CFR  Part 86)  is the  only test
     which  is  recognized  by the U.S.  Environmental  Protection Agency
     for  the  evaluation  of  vehicle  emissions;.    The  Federal  Test
     Procedure  and  the Highway  Fuel Economy  Test  (40 CFK  Part 600)
     are the  only tests which  are  normally  recognized by the U.S. EPA
     for  evaluating  .vehicle  fuel   economy.   Data  which  have  been
     collected  in  accordance  with  other  standardized  fuel  economy
     measuring  procedures  (e.g.  Society of Automotive  Engineers) are
     acceptable  as  supplemental  data to  the  Federal Test  Procedure
     and Highway Fuel  Economy  Data  will be used, if provided, in the
     preliminary  evaluation of  the device.   Data  are  required from
     the  test  vehicle(s)  in  both   baseline  (all  parameters set  to
     mamif-icturer's specifications)   and  Tr.oclifi.ec!  forms  (with  D-.-.vico

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17. Conclus ions

    The Applicant  submitted no  test  data  to  justify the claim  that  the
    Bask products would improve vehicle fuel economy or reduce emissions.

    The  Applicant  markets  two  Devices  (products).   However,  marketing
    identification of each was not given.

    The  Applicant  claimed  two  conflicting  theories  of  operation  to
    explain  the Device's  effect.  The  Applicant  claimed improved  fuel
    economy by  both  simultaneously heating and cooling the fuel  air  mix-
    ture.

    Installation  (i.e.  painting)  of   the  device  on  an  installed  engine
    would be  difficult  due  to the inaccessibility  of  the entire  exterior
    manifold surfaces.
                            List of Attachments

Attachment A                      Letter dated January 20, 1981

Attachment B                      Aqueous  Insulative  Coating Compositions
                         '         Containing  Kaolin  and  Staple  Fibers,
                                  Patent 4,240,936  (provided with Attach-
                                  ment A)   .

Attachments C-l, C-2              Testimonial  letters  (provided with  511
                                  Application)

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                                                                 Attachment A
                               P.O. BOX 15113
                          CINCINNATI, OHIO 45215
                               (513) 769-6948
                                                      January 20, 198!
Kr. Merrill W. Ko^th
U.S. Environmental Protection Agency
Ann Arbor, Michigan W3105

Dear Mr. Korth,

In response to your letter of January 12,  1981. Yes, we still are desirous
of having an EPA evaluation of our product.

I did not answer your earlier letters because I had no additional infor-
mation about our product regarding internal  combustion gasoline  engines.
The enclosed data ( patent and testing ) describes an aqueous insulative
coating composition that has significant thermal resistance to heat
transfer in thin coatings. If you exa.;.iira-: the test data fron Dr. De'fitt.PS
you will note that the coating when applied  away from a heat source in
thin coats has the capability to release heat faster than normal. This
assumes that the high emissivity coating is  applied to a  low cinissivity sur-
face.Such could be the case with the intake  :nanifold. In  other words, when
the coating is applied to the exterior surface  of  the intake manifold,  we
are in effect creating a cooler fuel charge  which  gives better engine per-
formance and better fuel economy. The insulative aspect of the coating  has
application on the air cleaner housing. That is, the coating shields the
internal compartment heat away from the air  cleaner housing,again,keeping
the air cooler. There are other areas on an  internal combustion  engine  where
this coating has application. Perhaps, that  is  where the  EPA could  be of
help to us.                                                           •

If you need any additional information please contact  me  at any  tine. This
information about our coating has also been  submitted to  the National
Bureau of standards in V/ashington for evaluation.
                               Very truly yours,
                               William J. Henning
                               President, Bask Industries

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:aiieti otaces latent [19]
in)
[45]
4,240,936
Dec. 23, 1980
, >4]  AQUEOUS INSULATTVE COATING
      COMPOSITIONS CONTAINING KAOLIN
      AND STAPLE FIBERS

[75]  Inventxx:   William J. Henniax,220 Forest Ave,
                 Cincinnati, Ohio 45215

[7.1]  AppLNo.:  35,462

[22]  FUetL      May3, 1979

[51]  Int. CLJ		CO8L 1/28
,'52J  U.S. O. _		260/17 R; 106/163 R;
         106/193  R; 106/197 Q 106/303 B; 260/17.4 R;
                                  428/454; 42V537
[58};  FftW of Scare* .	.	260/17.4 R, 17 R;
•,.;-..-.....-    .      106/308 B.  193 R, 197 Q, 163 R
  •"-."-"    ' •" .        • • .
[56J-V.    '      Referwcts Cited
       .  . U.S, PATENT DOCUMENTS
  2,C&Z^96  12/1936
  2,333,023  10/1943
  2,475,634  .9/1949
  3,639,297   9/1972
           12/1974
            «/1973
            9/197S
                  Lcppi.
                                 	.. 260/17 3.
                                 	 106/3C8 B
                                 	 423/454
4. Ml.730
4.155,S37
Tboopeco
Balalinecc .
106/163 R
            3/1979
       FOREIGN PATENT DOCUMENTS
    569679  8/1977  U.S.S.R.		 106/193 R

            OTHER PUBLICATIONS
Chcm. Absts^.vol.  76:142567h, Cirboxymcthyl  Ccl-
lulcse-BtncJcr-Papca-, Mi!ov ct »1.
Chcm.  Absix,  vol.  83:}36152x.  High-Temperature
Hcat-IajuladngCompcn^'^n N5atcria], Dfbrov ct al.
Chcm. Absts., 83:149.423m. Trtauecnt of Silicate Min-
eral* for Paper Coating. Maiden.
The Cood. Cbcm. Diet.. 5tb Ed., p. 619.
Primary Examiner—Edwsrd M. Woodberry
Attorney, Agent, or Firm—Wood, Herron & EVBJU

[57]               ABSTFrACT
A liquSd multi-purpose coaling composition is disclosed
which has significant resistance to beat transfer. The
exiting oonrpositkro may be applied to many different
types of S43bs»aics inchkling wood, metal, concrete ajxl
other structural materials. The composition b a \vater-
bascd liquid ccmtaining principally kaolin, staple fibers
and a dispersing agent. Tbe coating compcsition and
artcks coaled therewith  exhibit excellent insulating
properties agjdnst beat and radiant energy. Consider-
able energy savings arid various economics are obtained
by  the iasulativc composition*.

              14 dfliars, No Drawings

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                                             4,240,936
                       1                                                      2
                                                     to be suitably employed as a paint or coating composi-
      AQLTEOUS JNSULATIVE COATING            tion.  Compositions containing  these essential irtgrcdi-
>  OMPOSmONS CONTAINING KAOLIN AND      crits have been employed to coat various surfaces and
               STAP1JE FIBERS                     such  coatings formed thereby  have been found to be
                                                   3 edcquatcly bonded to the substrate and capable of with-
    BACKGROUND OF THE INVENTIO?'}         standing environmental jtress without peeling or othcr-
 '•"n: art of coating compositions has been very well    wwc degrading.
  •:!opcd. Considerable effort has been devoted to the       ID a" alternative form of this invention, particularly
•vdopmcnt of protective au*J decorative layers which    to enhajicc the bonding strength of the coating compo-
.y be formed on numerous subs-trales of metal, wood  10 sition to n surface, p.;,i/trD for this M whether it is to be employed as a waB paint or in other
-  ::iition: .2,413^7^ 2,414,391r  2,4S«,756;  £509,599;    environments where a decorative effect is not esscntiaL
.57.673;- 2,372^52^ 2,8! U«3;. 3,2024 67;  3,239,475;       jn formulating tlx: cocapoiitkjns of this invention, the
.•V.'-U73;.-331»,53S,- 3,323.425:  3,51 V56;  3,836,495,-    ^0^ compojx^t b the cridcaDy essential component
        3^07,726 and RE27,093. Th* zvbove patents    to prov;dc &e insubtive capabnity necessary to obtain
, rvol rcpracnted to be the nxs! pert oca J patents, but 23 ^ ^^p^ of ^ invenUoo> ^^ fmounl rf fc|O,;I1
                                                                                 >
 : cornered to thsclo^ coatog compoatyoa which    ^^oy^ wilj vajy bot n substanlial ^nouni musl
             may be compared to the subject matter    __ »..  _. •  ,v   -_„_     _j-  :_ ~A~, »~
   .  .      .             *                            empioycu in tee djueous xncuui in orccr to
 f' n mvcn     ..             ,--.                     coating  which may be  film-formed  and msulating>
      SUMMARY OF THE INVENTION         30 Whereas kaolin  has been employed io prior coating
 .,_   .    ,  .        .          ..    f ..,•  -     •      compositions, it boot fcr.own by npplicant to Jiave been
 17:c insulatrve coating compcsjtjoo of thb invention        f   ...     •  „  ,                ,  .    .
           ...  • ,.  ,-     .^_i    .   «  r-u      j     employed LO substantially large amounts such that the
 r.si5.ts essentially of kaolmpartjcies, staple!fibers and a        .     . ..._,/    ,     -          -  r,    r
             , -         *      • ,-    i. •>    v.       coating  wh>clj B firrn-formcd coasjstj essentially of
         agcol m aa aqueous medium. It has been    .,..,._„              ,,          .
                                                     —-•••-•— kaoho. Therefore, amounts of jcaoun on the
 i rxl that a highly efficient msu^trvc coating coinpcsi-
 n'nwy be formulated in * rkjrad state having a VBCC*- X  ?rdcT of about ™fo ">»« 9°% by weight are employed
  wluch makes it easily employed w a paint composi-   ' cl ^c«x« ?»*» to acrocve the cleared results. AJV
   or a multi-purpose coating. Tb* compositJct. has     olh€r °^^' component ts the fibrwts binder. It has            t
                                                      been found that cellulose fiberj, made from shredded
                                                                                                                     j

  n found to provide substantial resistance to transfer     bcca touDd thal ccU^'ose fibers, ni3c5c from ^redded             *
^ heat or radiant energy. The composition can be very     newspaper wh>cb ha* been blended m the sq^ota me-            ^
ronotnkalJy formulated to provide an energy saving 4Q  di^ wch thal tfte fib=rs »«»me dispersed  therein, arr
 •ating. la thb connection, h ha*been discovered that     suable. In general,  staple fibers, Le.. on an order of
-: ides such as walls, window frames, light futures, and     magnitude of about J irjcb to about 2 inches, enable the
 c  !.:ke ca» be  provided with * coating which  win     coating  composition to be applied satisfactorily to a
 .;.b!c insulatrve properties to be enhanced on sJgnifi-     surface.  The fibers permit the aqueous kao'.ir. coating
int orr!ers of magnitude even with rdativdy thin coat- 45  composition to be film-formed on a surface ar,d bound
. ^  layers.                                              thereon  without cn>cking. In other words, the fibers
 in a preferred form, the msulative ooatrng composi-     serve an essential binding function oa the kaolrn solids
 m consists essentially of an aqococa medium contain-     which arc film-formed on a surface. The ceUnlose fibers
 .;;  rJm-forming solids consisting e&senttally of a  sub-.    *&*> provide a supplemental iraul.iting capability, dc-
 ..itial amount of kaolin, c minor amount of cellulose 50  pc"d'ng uP°n  the quantity  employed'b the composi-
  -: s and a minor amount of a dispersing agent In this     tion. Generally, reinforcing staple fibers arc included on
  p.position, it has been found that the kaolin may be     8TI order of about 1  to about 5 percent by weight. It
  .1 i'erroed onto s surface and provide a significant     should be understood that the so called "slapk:" fibers
 u 1'ating capability. The effects arc considered to be     vary in  length, but arc normally short fibers and these             \
 .-prising and heretofore unappreciated. Also, thecoat- 55  a^c preferred.  Whereas,'it is also prefcrabVe to employ             I
 ..-. niay be subjected to environmental, as well as ex-     ccllulosic fibers because they arc relatively inexpensive,
 .•n)c ambient stress conditions, and the coating will not     and such fiberj rwve been found tocoact with the kaolin
 .•'.ok. peel or powder. In thb composition, the cellulose     clay to provide the desired results, it should be undcr-
 -:-rs  may be very economically  provided by waste     stood that other fibers of a similar nature including-
 ifxrr or newsprint which  ha*  been  shredded  and 60  cotton, wool, wood, glass, polyester, or the like may be
 rrsdcd with the kaolin and dbpersing aids.              employed to provide the desired results according to
 hi  another preferred form, the insulstive coating     the principles of thb invention. However, for econo-
 •i!position b formulated with kaolin in » substantial     mica and  energy savings,  waste paper fibers arc pre-
   •••!Mf to provide insulating capability, cclluknic fibers     ferrrd.
   x:r.!nr- amount, dispersing aids and a thickcrin^ or  63    Dbpersants  are employed  in  the ao4!j5O'j-s  ceat-.ng
  .;.(!Op;c agent in s minor amount Thb fonr.ulation     compositions to adequately iujp«xj JJ>d  stabilize the
 . :niLs the crap'oyrncnt of amounts of insuhtiw; kaolin     kaolin particles  in the aqueous media  along with the
 .ty,  ^dequately dbpcrsed »nd stabilized  in a liquid base    binding ccllulosic fibers and other additives. Such

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                        3   •                   ^40,936         I'-'         ^

 •  •.::;; agsnU or surfactaios are well known and devcl-    reference to the above mentioned pjicriis. U'hcn em-
 .-.! in the coating art. Typically, the surfacLjii!! arc of    ployed, depending upon ihc desired effect, such laliccs
 •  -inionic type- Inorganic anionic surfactants or dis-    arc used in amounts of from sboul 5 to about 20 percent
  ;ing aidi inclixle  tctrn potassium pyro phosphate,    by weight. In compositions of thts invention, an acrylic
   :r alkali metaJ phosphorus salts, or other alkali or  3  resin, a poly vinyl aceintc or copdy-mers thereof arc
  • line earth metal  salts. Other anionic surfactants    preferred.
 iuJe alkali and alkaline earth metal salu of ncutral-
 .! phosphoric  acid eaters of oxyalkylated higher alky!
  nob or aliphatic monohydric alcohols. Other ani-
 ic surfactants of saponified fatty acids or scaps arc  10
 •!! known in the coatings  art and rcfercrvce may be
 •.tie to the above patents for further detulj of such
 parsing aids or surfactants. In general, a surfactant or
 ;/rrjJng aid is employed in  a minor amount, i.e., on an
 .\r.r of about 0.01 to about 1.5% by weight.  In  nddi-  15 general rule.
 •:: to the ankmvc dispersing aids or surfactants, non-       The principles of this invention V--H1 be further undcr-
 :ic agents may also be employed. Typically, the non-
 ••c  surfactants  have  hydrophilic  portions  or side
 •ijns usually of the polyoxyalkylene  type.  The oil
 iublc or dispcrsabre  part of the molecule is derived 20
 >-n either fatty jxrxis, alcohols, amides or amines. By
 .:i:iblc choice of starting materials and regulation of
 : length of the polyoxyalkyleoc chain, the surfactant
 .. u of the DOniocuc detergents may be varied as b well
 ..nvn. Suitable examples of nonionic surfactants in- 25
 :-.!c alkyl pbenoiy polyoxy cihylcnc gjyco*. for cxaro-
 ••:, cthylene oxxie adduct of either octyl-, nonyl- or
 .!ccyl plienoi arxJ the like, Tbese mentioned ivonionic
 i inctantj arc usually prepared by reaction of the alkyl
 ' c-nol with ethyVene oxide. Other anionic or DOnionic 3O
 •r-^rsants or surfactants which may be employed and
                                                         Other ingredients, such as funjpckics may  also be
                                                       included. Among the suitable pigments which  may be
                                                       used in accordance, with this invention  are  the finely
                                                       divided ruti'c tiunium dioxides. Plainer.;* other than
                                                       rutilc lit.inium d>oxidc can, however, also bo  uicd The
                                                       pigment particles should not have * diimctcr in excess
                                                       of about 50ft, bul particle sizes cvca «j little as. 0.1  arc
                                                       suitable. The particle siies of the tao4in follow the same
                                                       stood with reference to the following

                                                                           EXAMPLE I
                                                         An insulative coatiog composition was prepared by
                                                       blending the following ingredients


                                                           Perccol
                                                            42.6*
                                                             .14
                                                             .43
                                                             .43
                                                             J&
                                                             Z13
                                                                     Trtn PotauiiTO 1
                                                                     (Sertactanl ex Cnpcru>( Aid)
         Wetting A^cnl (P)yr*c*A '
         LccJuitrin (Pijmcni 1
         EUiyiCT* Glyoo! (Motsr^nr Xcteoc
   well known in the coating formulation art arc dis-
..vcd, for example, in "Surface Active Agents  and
         s^-by Schwartz ct al (1958, InterscicEcc Pub-
                       '    ,.:....   -    •        •     35
  •V'h-en the loolin b employed in a substantial jxnxxmt
 che aqueous media, for cxampie 70 percent by •weight,
 ;::n'Js to have its own thixotropk: properties. Accord-
 . ;!y, the coating composition may be so formulated at
 •oh high solids concentrations of kaolin and the viscos- 40
 y is such that it may be readily applied aa a paint or
 ••Ming. However, at lower concentrations of kaolin,
 •r example about 3O-4Q%, it may be necessary to cm-
•'oy  a thickening agent. Thickening  or  thixotroptc
 .ents such as bydroxy ethyl cellulose, metliyl ccllu- 45
 •-c. carboxy tnethyj cellulose therefore may be em-
 'oyecl in a very minor amount on  the order of about
 '>!  to about 13% by weight. Other thickeners which
...iy be used are polyvinyl  alcohol, gum arabic, gum
                                                             1.42
                                                              .43
  .07
 3.13
 4.26
 3.5J
30.70

  jcn

 9J4
 100
         Butyl Eih« of Dict^fepc CJycol
         Acrtalfi (Co*icx3ni A£n>*im O>OJ:.'~
                                                                           i Cii) :;
                                                                     ICtoln (P>rricic Sire
                                                                            ^urfr 0.1
                                                                     \'nj1 AccCt:c Acrjlic
                                                          The above composition was formulated for painting
                                                        interior surfaces. The kaolin compor>eT>t was contained
                                                        in a high percentage on a dry weight basis and the ccllo-
                                                        losic fibers  were provided  by  shredded  newsprint
         , ammonium polyacrylate, sodium polyacryl- 50  which was dispersed throughout tbc aqueous media
 ;•, .v.::moniuro alginatc, sodium alginatc. and the like.     during high sp-ecd blending. In thts fonuuLttkMi s vinyl
 As MJO mentioned, when desired, a polymer or latex     acetate acrylic copolymcr latex is i»ed to provide addi-
  drr may be employed to serve as a supplemental     tional binding strength of the cc-itinj oo the wall sur-
 • •.':cf :'.nd aid in the adherence of the coating composi-     face. The other ingredients and their fuoctioo arc identi-
  :i to a. surface. Conventional latex polymers are usu- 55  fied in the above listing of the coffipoocnis.
 ''.••> thermoplastic.  The polymer particles arc made     •  The composition of Example 1 was coated oclo the
 :!icicntly soft or additives are included in the formula-     interiors  of aluminum window  fr»n>cs. The  coating
 • :n to permit ccudcsence of the particles as a film after     composition was applied  with a brush on an unpaintcd
: is formed. Polymers and copolymers of acrylic acid.     aluminum interior window frame ra a thickness of ap-
 ic-lhacrylic acid, esters of these acids, etc.,  generally 60  proximatcly 4-6 mils, Widi an outsxSe air tenperaturc
.'.lied an "acrylic  resin** are usually employed. Viny-     of about 40* F. and an indoor temperature of sbout 65*
•crlnte and cthylene copolymers are also employed in     F., the window frames coxted with the iosulabvc com-
.-.oh  laticcs. Among other water dispersible binders arc     position exhibited a temperature of »boot 55" F. The
• :lyvinyl alcohol, hydrol>-zcd polyvinyl acetate, hy-     temperature results were obuined using » Raytex Infra-
   '.VT.td copolymers of vinyl esters or organic acicJi  65  red Scanner No. R3SORVF. hiving an sccvr^y of pli:.i
 ••.'•  other  po'iyrr-icmiblc comonomcrs, for example,     or minus2* F. Tl>e ur«ro.i!e-J v.indow fruixv* in ihc s.i:n tcmt-xrjturc  rr^xiinj  of 62' F. The
 •.r. Other polyrr>cT based laticcs may be employed with     temperature  reading on  the puCoCe frame thai w.is
                                                                                                            1.
                                                                                                            *.''•
                                                                                                            8
                                                                                                             I
                                                                                                             1
                                                                                                             V
                                                                                                             5
                                                                                                             j-
                                                                                                             i

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                                                                    1J
                                                4,240,936
coated on the interior frame with the irwuhlive coating
Composition was about 53' F. The temperature on the
outside frame that was not coated on the interior fnime
was' about 60"  F. Accordingly, -the insulativc coating
composition of this invention when applied to such an  5
aluminum substrate provided about a 10 to 12% reduc-
tion in heat lo?.v                     •  • '.   / '
  In order to further demonstrate the insulative charac-  '
tcrislics of a coating composition formed In accord :\r>cc
with the principles  of Lhk» invention, z. 9 jr-ch length of  1°
} inch OD copper tubing  waa  :x«ited with approxi-
mately a 1 inch thjckjxss r-f tlic insulative coating cora-
ncsiuon of Example • 'ioto one end of the tubing for 5
ii,ch~ T..--  _.uve o^tiag was applied with a brush
                                                                                6
                                                                            -continued
                                                           Percent
                                                                     Ingredient
                                                             2.55     Ethylerx Clycol
                                                             1.70     Butyl EiScf of D>eihylcr« Clycol

                                                              .51     Chethylew: Gl>col Ethyl Elh«r
                                                              .C3     Bx:letTckJe-Fun£Jov<= « Formica, top table having a .medium brown
                                                        color in a room heated at about .63' F. Prior to coating
                                                        the rcfkcti ve shield  with the above composition, the
                                                        1'ght ^^ turned on for aboul one hour. "There  was no
                                                        temperature change observed upon taking readings of
                                                        the uble surface upon employing the infrared scanner
                                                        described  in Example I. However, after coating the
                                                        reflective shield of the lighting fixture using the coating
                                                        composition of this Ej^unptc II, the temperature read-
                                                        ing on the table was about 67" F. after one hour with the
\vilh Example I was also applied to walls, ceilings and  30  light. The room temperature remained at 63"  F. The
lloorx with suitable applicators in thicknesses approxi-
mating about  10-12 mQs. After a passage of about  6
months, the coating did not chip, peel or powder. Fur-
thermore, such coatings applied to heating ovens have
exhibited considerable natural gas savings. For Lastar.ce,
the interior of a large Lodortrial baie oven was coated
on its walls, ceiling and floor with the composition of
Example I having a thickrvess approximating 10-12 mils.
This coating after six months has not chipped, peeled or
powdered. Prior to coating the industrial bake oven, a
start-up of the oven up to the oven temperature of 3CO"
F. required about 55 minutes. After coating, only 30
minutes were  required to come up to 300" F. Addition-
ally, the following temperature readings were taken at
four different  locations on  the exterior of the  insulated
oven booth, both before s.rxJ after the coating was ap-
plied.


Ccxiirol Area
(Vinho'c Am
Main Acccu
Ke«r Acco> Ethvl Ctllulfw
Cctlulmc FiSrr
    Pcrccul
                                                     65
     16,16
              Tctm
              Anti-foam
                           Pyro
  The above formulation was essentially the same as
Example II,  except  that the Isles binder,  coalescing
agents and pigment were eliminated. When th: formula-
tion was employed to co-'it various surfaces in a manner
substantially similar to the coating of articles according
to Examples 1 and H. substantially similar results of
insulalive and reflective capabilities were achieved.

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                         /                                                        o
  :\ .-."C'.jrriar>cc with the above description and operat-      8. The composition of claim ~l wherein said
  ••/..::•.pier, other medifications may be uiide to this     fibers arc derived from wist; paper.
,  .:,,:ion  without departing from the spirit a/>d scope      9. An aqueous insulati^c coating composition having
•,-.<.•<:> f.                                                  film-forming solids consisting essentially of kaolin parti-
 : chum:                                             5  clcs in an amount of about 30 to about 90% by weight.
 '. An imvliijve aqueous coating composition con-     waste paper fibers in an amount from about 1 to  about
••'.irr< film-forrniag solids consisting cSMmtLxlly of tao-     59o by weight and a minor amount of a dispersing agent
.  ; articlw in an amount on the order of about 30% to     for said  solids in  the aqueous composition,  said kaolin
 -.".it  90% by weight,  itaplc fibers  and a dispersing     panicles having a diameter less than about 50 microns.
 • :it for  laid solids  in the aqueous composition, said  10   10. The composition of claim 9 wherein said dispers-
 ,,lin  particles having a diameter less  tha-n  about 50     ing agent is selected from the group consist!-!:; of non-
 ::rons.                                    "            ionic and anionic surfactants.
 .'•:. The composition of claim 1 further comprising a      11. The composition of claim 10 wherein said dispcrs-
:• 'xcnin^ agent.                                         ing agent is present in an amount of from about 0.01  to
 ..V The composition of claim 2 -wherein said thxrk-en-  15  about 1.5% by  weight
 ; ar,tnt  U a cellulcsic thickcjvcr.                          12. The composition of claim 9 further comprising a
  '-. The composition of claim 3 wherein said ocllulosic     ccllulosic thickener in an amount of from about 0.01  to
 o!c.r;>er is selected from the group of methyl cellulose,     about 1.5% by  weight
,..1,'oayethyl cellulose and carboxymethyl cellulose.        13. The composition of claim 9 further comprising a
 :>. Th« composition of claim 1 further comprising a 20  btei binder in an amount of from about 5 to about 20%
•::>or  amount of * btci binder.                           by  weight
 &. The  cocjpcwtiofl of Ha>m  5 wherein said  latex      14. The composition of claim 13 wherein said late*  **A
i-icJ-r  M selected frotn the group of an acrylic resin, a     binder  is  selected  from  the group  consisting  of an  vT-rTj
nyl acetate polyrocr, and copoJymcrs thereof.            acrylk: resin, a vinyl acetate polymer and copolyrrtcn
 7. The composition ofdaicn 1 wherein said  fibers arc 25  thereof.
        fibers.    '  •                                                       .....
Vv».
<;*
                                                    35
                                                     <5
                                                     50
                                                     60
                                                     65

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    ,,  ,  CINCINNATI Yi;i.LOW CAR CO.. INC
   ...'.:.2..L:.x  mnxi Muior.               PARKWAY TAXI CO...
       January 3,
       it r .  \-'. i 1 1i a in J .  H e n n i n g
       P. a s k T11 d u s t r i o r., I n c .
       P.O.  Hox 15113
       Cincinnati, Ohio    V5215

       Dear Hr. Henning:

       The  fo.llovn'.Mg are results  v.-hicli  v?e could detect from  the
       Bar.kotc  coating which was  applied to three of our vehicles.

       The  firr.t  reoult was the detor-iorntion of heat luii "I.d-up
       from v/ithin the engine conipr-.rtiaent.   Thi.-: :i n our industry
       could be of very f.rent import.p.nce by cre;itin{- a longer engine
       .VJfe plus  giv.inp; nc: additional v;are fr-orr, the he To 5; and hoses
       necessary  for the operation  of our vc.-hicler..

       The  next result war. a slight  increase :i n the gasoline mile-
       age.   We noticed approximately one (I) mile per gallon increase
       on an average.  .The effect, of Baskcto on gasoline nixleago  i:; a
       difficult  one for UK to determine due to two main factors;

          1)   The age of  the vehicles  which were used in the test
               and the fact each  had over 100,000 miles.

         i?)   The driving habits of the various drivers which  were
               ope r- a t i. n g t h o v e h i c 1 e s d u ran g the t e :> t period.

       The  results received froir>  our testing of Haskote could be  of
       great b(Mu?f.it to our industry.
       ;'J.  Cahall, President
       Cincinnati Yellow Cab  Co.,Inc
  (jy.,v  Parkway Tasi. Company
1110 Kl NSI l{ SIKIT1
CINCI-^.SAII. OHIO -»S

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 December 17, 1979
 Mr.  William J. Henning
 Bask Industries
 P,  o. Box 15113
 Cincinnati, Ohio  45215

 Dear Mr. Henning:

 For your records,  on the four trucks  involved, we
 experienced, during the s.uirtmer months,  an  honest'.3/10 of
 a. -mile. improvement on fuel economy.

 We  weren' t sure of the. effect of cold weather on these
 'ye.hficles-, but  to  da.te we have not noticed  any drop in
 .fuel economy w.hile. operatincj in cold  temperatures.

 Your- product,  Basko, se.ep.s- to afford  an excellent heat
• s.hi.eld from encjirxe temperatures.
    W.. Hea.drick
          of -Maintenance
    : be
         4560 N. Second St. St. Louis. Missouri 63147 (314)231-0350

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