&EPA
            United States
            Environmental Protection
            Agency
                Office of Mobile Source Air Pollution Control
                Emission Control Technology Division
                2565 Plymouth Road
                Ann Arbor, Michigan 48105
EPA 460/3-87-002
June 1987
            Air
Study of the Effects of Reduced
Diesel  Fuel Sulfur Content
on Engine Wear

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                                             EPA 460/3-87-002
Study of the Effects of Reduced Diesel Fuel
        Sulfur Content on Engine Wear
                           by

                      Edwin A. Frame
                      Ruben A. Alvarez
                      Norman R. Sefer

                  Southwest Research Institute
                     6220 Culebra Road
                   San Antonio, Texas 78284

                   Contract No. 68-03-3353
                    Work Assignment B-1

               EPA Project Officer: Craig A. Harvey
                        Prepared for

             ENVIRONMENTAL PROTECTION AGENCY
            Office of Mobile Source Air Pollution Control
              Emission Control Technology Division
                     2565 Plymouth Road
                  Ann Arbor, Michigan 48105
                        June 1987

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This report is issued by the Environmental Protection Agency to report technical data
of interest to a limited number of readers.  Copies are available free of charge to
Federal employees, current contractors and grantees, and nonprofit organizations - in
limited  quantitites -  from  the Library Services  Office,  Environmental Protection
Agency, 2565 Plymouth Road, Ann Arbor, Michigan 48105.
This report was  furnished to  the  Environmental Protection Agency by  Southwest
Research Institute, 6220 Culebra Road, San Antonio, Texas, in fulfillment of Task f in
Work Assignment No. B-l of Contract 68-03-3353.  The contents of this report are
reproduced herein as received from Southwest  Research Institute.  The opinions,
findings, and conclusions expressed are those of the author and not necessarily those of
the Environmental Protection Agency.  Mention of company or product name is not to
be considered as an endorsement by the Environmental Protection Agency.
                        Publication No. EPA-460/3-87-002
                                       11

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                                 FOREWORD

     This project was conducted for the U.S. Environmental Protection Agency by the
Division of  Fuels and Lubricants Research, Southwest Research Institute.  The project
was to complete Task 4 as authorized by Work Assignment B-l  under  Contract 68-03-
3353.  Work was initiated  September  2, 1986, and completed in June 1987. It was
identified within  Southwest Research  Institute as  Project  08-1193-001.   The EPA
Project  Officer was  Mr.  Craig A. Harvey,  and the Branch Technical Representative
was Mr. Timothy Sprik, both of the Emission Control Technology  Division, Ann Arbor,
Michigan.  The  SwRI project  team included Mr.  Edwin A.  Frame, Mr.  Ruben A.
Alvarez, and Ms. Margaret B. Millikin.  Mr.  Norman R. Sefer was project manager and
was involved in the initial technical and fiscal planning.
                                       111

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                                  ABSTRACT

     The study evaluated wear in heavy-duty  highway-type engines for  reduction of
sulfur content  of diesel  fuel  in  the  range of 0.50 weight  percent to 0.05 weight
percent.   A  literature review  found that  wear  rates  generally  were reduced by
decreasing fuel sulfur content.  The amount of wear reduction was affected as much
by operating  temperature and  engine  load  as  by sulfur  in the fuel.  Low  operating
temperatures showed more wear at high sulfur levels and, therefore, more benefit for
low sulfur fuels. Increasing engine load caused higher wear rates independent of sulfur
content.  Lubricant alkalinity (Total Base Number) is effective in controlling corrosive
wear at high sulfur levels and reduces the potential wear benefit from low sulfur diesel
fuel.  Lubricating oil analyses from fleets operating on diesel fuel with less than  0.05
weight percent sulfur were compared with previous data  when average sulfur content
was 0.35 weight percent.  Overall, a significant  reduction in engine wear occurred in
most engine types as measured by iron content of used  oil. Most of the reduction can
be attributed to  the low sulfur fuel, with minor  contributions from changes in the
lubricating oils.
                                      IV

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                           TABLE OF CONTENTS

Section                                                                 Page
FOREWORD 		-	-	     iii
ABSTRACT	-	     iv
LIST OF FIGURES 	-	     vi
LIST OF TABLES		-				     xi
SUMMARY 		-	-	.—    xii

1.   INTRODUCTION 				-	      1

     1.1   Background 	      1
     1.2   Objective	      1
     1.3   Approach	      1

2.   LITERATURE REVIEW —	-			-	-	      2

     2.1   Introduction  	      2
     2.2   Discussion of Literature 	      3
     2.3   Comments on SAE Paper No. 700892 	     21
     2.4   Engine Manufacturers 	     21

3.   FLEET DATA ON ENGINE OIL ANALYSES  		     23

     3.1   Initial Contacts With Fleets	     24
     3.2  Southern California Rapid Transit District Fleet	     24
     3.3  Chandler, Suppose-U-Drive (Rental Trucks), and Laidlaw
             School Bus Fleets 	     39

ft.   CONCLUSIONS AND RECOMMENDATIONS  		-	-     64

     4.1   Conclusions From Literature Review 	     64
     4.2  Conclusions From Fleet Data	     72
     4.3  Recommendations	     72

5.   REFERENCES 	-	     74

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                              LIST OF FIGURES


Figure                                                                    Page

   1.   Effect of Fuel Sulfur Content on Piston Ring Wear QO)  	      7

   2.   Effect of Fuel Sulfur Content on Engine Wear (5)  	      8

   3.   Effect of Fuel Sulfur Content on Cylinder Bore Wear UO)  	      9

   4.   Effect of Fuel Sulfur Content on Cylinder Liner Wear
           With Engine Oil 1 08)  		-		     10

   5.   Effect of Fuel Sulfur Content on Cylinder Liner Wear,
           Engine Oil 1 with Anti-Corrosion Additive (18)  	     11

   6.   Relation Between Fuel Sulfur Content and Ring Wear, Single-
           Cylinder Four-Cycle Diesel Engine  	     12

   7.   Wear Rates with Reduced Sulfur Content  	     13

   8.   Effect of Jacket Temperature on Piston Ring Wear with
           Fuels of Different Sulfur Content 	     14
   9.   Effect of Jacket Temperature on Bore Wear with
           Fuels of Different Sulfur Content  	
  10.   Piston-Ring Wear Related to Coolant Temperature in a
           Two-Stroke Diesel Engine (Unknown fuel S level)  	     15

  11.   Effect of Fuel Sulfur Content and Jacket Temperature
           on Engine Wear (5)  	     16

  12.   Top Compression Ring Chrome Face Wear Rates for
           Cummins VT-903	     17

  13.   Effect of Load on Top Ring Wear Rate as a Function
           of Outlet Coolant Temperature   	     18

  14.   Effect of Load (BMEP and Peak Pressure) on Bore
           Wear Rate  	     18

  15.   Low-Temperature Corrosive Wear is Reduced by Use of
           Alkaline Lubricating Oil Additives	     19

  16.   Corrosive Wear is Reduced Through Use of Alkaline Oil	     19

  17.   TBN/TAN Versus Oil Miles	     20

  18.   Comparison of ASTM D 664 and ASTM D 2896 TBN Analyses  	     20

  19.   SCRTD Fleet, Sulfur Content of Diesel Fuel, Trailer and
           and Tank Samples 	     28
                                      VI

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LIST OF FIGURES
   (Continued)
Figure
20.
21.
22.
23.
24.
25.

26.

27.

28.

29.

30.
31.

32.

33.
34.

35.

36.
37.
38.

SCRTD Fleet, Sulfur Content of Diesel Fuel, Annual Average 	
SCRTD Fleet, Average Oil Miles 	
SCRTD Fleet, Average Iron Content of Lubricating Oil 	
SCRTD Fleet, Average Total Base Number of Lubricating Oil 	
SCRTD Fleet, Average Oil Miles (CUV903 Engine) 	 - 	
SCRTD Fleet, Average Iron Content of Lubricating Oil
(CUV903 Engine) 	 - 	 	
SCRTD Fleet, Average Total Base Number of Lubricating Oil
(CUV903 Engine) 	 	 — 	 	 	
SCRTD Fleet, Average Oil Miles of Lubricating Oil
(DDV71 Engine) 	 	 — 	
SCRTD Fleet, Average Iron Content of Lubricating Oil
(DDV71 Engine) 	 	 —
SCRTD Fleet, Average Total Base Number of Lubricating Oil
(DDV71 Engine) 	 	 ~
SCRTD Fleet, Average Oil Miles (DDV92 Engine) « 	 - 	
SCRTD Fleet, Average Iron Content of Lubricating Oil
(DDV92 Engine) 	 - 	 - 	 	 	
SCRTD Fleet, Average Total Base Number of Lubricating Oil
(DDV92 Engine) 	
SCRTD Fleet, Average Oil Miles (MAN866 Engine) 	
SCRTD Fleet, Average Iron Content of Lubricating Oil
(MAN866 Engine) 	 	 - 	 - 	
SCRTD Fleet, Average Total Base Number of Lubricating Oil
(MAN866 Engine) — 	 - 	 - 	 - 	 -
Chandler Truck Fleet, Average Oil Miles 	
Chandler Truck Fleet, Average Iron Content of Lubricating Oil 	
Chandler Truck Fleet, Average Zinc Content of Lubricating Oil 	
Page
29
30
30
31
33

33

34

34

35

35
36

36

37
37

38

38
41
42
42
        vu

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                               LIST OF FIGURES
                                  (Continued)
Figure                                                                      Page

  39.    Chandler Truck Fleet, Average Oil Miles (Caterpillar Engine) 	      45

  40.    Chandler Truck Fleet, Average Iron Content of Lubricating Oil
           (Caterpillar Engine)	      45

  41.    Chandler Truck Fleet, Average Zinc Content of Lubricating Oil
           (Caterpillar Engine)	      46

  42.    Chandler Truck Fleet, Average Oil Miles (Cummins Engine)	      46

  43.    Chandler Truck Fleet, Average Iron Content of Lubricating Oil
           (Cummins Engine)  	      47

  44.    Chandler Truck Fleet, Average Zinc Content of Lubricating Oil
           (Cummins Engine)  	      47

  45.    Chandler Truck Fleet, Average Oil Miles (Detroit Diesel Engine)  —      48

  46.    Chandler Truck Fleet, Average Iron Content of Lubricating Oil
           (Detroit Diesel Engine)  	      48

  47.    Chandler Truck Fleet, Average Zinc Content of Lubricating Oil
           (Detroit Diesel Engine)  	      49

  48.    Chandler Truck Fleet, Average Oil Miles (Mack Engine) 	      49

  49.    Chandler Truck Fleet, Average Iron Content of Lubricating Oil
           (Mack Engine)	      50

  50.    Chandler Truck Fleet, Average Zinc Content of Lubricating Oil
           (Mack Engine)	      50

  51.    Rental Truck Fleet, Average Oil Miles 	      51

  52.    Rental Truck Fleet, Average Iron Content of Lubricating Oil  	      52

  53.    Rental Truck Fleet, Average Zinc Content of Lubricating Oil 	      52

  54.    Rental Truck Fleet, Average Oil Miles (Cummins Engine)	      53

  55.    Rental Truck Fleet, Average Iron Content of Lubricating Oil
           (Cummins Engine)  	      55

  56.    Rental Truck Fleet, Average Zinc Content of Lubricating Oil
           (Cummins Engine)  	      55

  57.    Rental Truck Fleet, Average Oil Miles (Detroit Diesel  Engine)  	      56
                                       via

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                               LIST OF FIGURES
                                   (Continued)
Figure                                                                      Page

  58.    Rental Truck Fleet, Average Iron Content of Lubricating Oil
           (Detroit Diesel Engine)  	      56
  59.    Rental Truck Fleet, Average Zinc Content of Lubricating Oil
           (Detroit Diesel Engine)  	      57
  60.    Rental Truck Fleet, Average Oil
  61.    Rental Truck Fleet, Average Iron Content of Lubricating Oil
           (Deutz Engine)	      58

  62.    Rental Truck Fleet, Average Zinc Content of Lubricating Oil
           (Deutz Engine)	      58

  63.    Rental Truck Fleet, Average Oil Miles (CMC Engine)	      59

  64.    Rental Truck Fleet, Average Iron Content of Lubricating Oil
           (CMC Engine)  					      59

  65.    Rental Truck Fleet, Average Zinc Content of Lubricating Oil
           (CMC Engine)  	-		      60

  66.    Rental Truck Fleet, Average Oil Miles (Inter-Harvester Engine)  	      60

  67.    Rental Truck Fleet, Average Iron Content of Lubricating Oil
           (Inter-Harvester Engine) 	      61

  68.    Rental Truck Fleet, Average Zinc Content of Lubricating Oil
           (Inter-Harvester Engine) 	      61

  69.    Rental Truck Fleet, Average Oil Miles (Caterpillar Engine)  	      62

  70.    Rental Truck Fleet, Average Iron Content of Lubricating Oil
           (Caterpillar Engine)  	      62

  71.    Rental Truck Fleet, Average Zinc Content of Lubricating Oil
           (Caterpillar Engine)  	      63

  72.    Laidlaw School Bus Fleet, Average Iron Content of Lubricating Oil  ~      66

  73.    Laidlaw School Bus Fleet, Average Zinc Content of Lubricating Oil —      66

  74.    Laidlaw School Bus Fleet, Average Iron Content of Lubricating Oil
           (Cummins Engine)	      67

  75.    Laidlaw School Bus Fleet, Average Zinc Content of Lubricating Oil
           (Cummins Engine)	      67
                                       IX

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                               LIST OF FIGURES
                                  (Continued)
Figure                                                                      Page

  76.   Laidlaw School Bus Fleet, Average Iron Content of Lubricating Oil
           (Detroit Diesel Engine) 	      68

  77.   Laidlaw School Bus Fleet, Average Zinc Content of Lubricating Oil
           (Detroit Diesel Engine) 	      68

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                               LIST OF TABLES
Table                                                                      Page

   1.   Attitude of Diesel Engine Builders Relative to Sulfur
           Content of Diesel Fuel  	      22

   2.   Average Iron Concentration, ppm, for Southern California
           Rapid Transit District Fleet  	      27

   3.   Comparison of Fuel Sulfur Content For Southern California
           Rapid Transit District Fleet  	      28

   4.   Comparison of Selected Data For Southern California Rapid
           Transit District Fleet   	      29

   5.   Comparison of Selected Data for Southern California Rapid
           Transit District Fleet  By Engine Type   	      32
   6.    Comparison of Selected Data For Chandler Truck Fleet
   7.    Comparison of Selected Data For Chandler Truck Fleet By
           Engine Type	
   8.    Comparison of Selected Data For  Rental Truck Fleet	      51

   9.    Comparison of Selected Data For Rental Truck Fleet
           By Engine Type  	      54

   10.    Comparison of Selected Data For Laidlaw School Bus
           Fleet (Total Fleet)  				      65

   11.    Summary of Fuel Sulfur Effects 	      69
                                       XI

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                                   SUMMARY

     The effect of diesel fuel sulfur content on wear in heavy-duty  highway diesel
engines was studied in  a two-phase approach. In the first phase, a literature review
investigated the role of sulfur content in engine wear as affected by engine operating
conditions and lubricating  oil quality.   Information was  also obtained  from diesel
engine manufacturers.  In the second phase, data were obtained from four fleets in
Southern California operating on diesel  fuel containing less than 0.05  weight percent
sulfur.   Sulfur content of diesel  fuel  was  controlled  at  that  level  by regulation
effective January 1,  1985,  in the South Coast Air Basin which includes Los Angeles,
Orange, Riverside, and  San Bernardino Counties.  Diesel fuel and used lubricating oil
analyses before and after the change were compared in a statistical evaluation.

     Fuel sulfur content effects on corrosive engine wear were reported extensively
in the  literature.   Data obtained with modern engines and lubricants  were the most
applicable, particularly in the 0.50 to 0.05 weight percent sulfur range.  The main
findings were:

     •    Reduction of fuel sulfur content results  in less  engine  wear  at  some
           conditions.
     •    Wear reduction is greater below the normal operating temperature of about
           175°F.  Therefore, the benefit for low sulfur fuel depends on the amount of
           time the engine would operate below normal temperatures.
     •    Higher engine load increases the amount of wear, independent of sulfur
           content.
     •    Operating temperature, engine  load,  and fuel sulfur content appear  to be
           equal in importance as factors in engine wear.
     •    Lubricating  oil alkalinity (Total Base  Number) controls engine  wear at high
           sulfur levels and reduces the potential wear benefits from low sulfur fuel.
     •    Lower  sulfur fuel may allow  longer  oil change intervals  by less  TBN
           depletion if  other oil contaminants are not controlling oil changes.
     •    Reduction in engine wear from low sulfur fuel may not extend life if other
           failure modes are controlling the need for engine overhaul.
                                        xu

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     Data from one fleet showed that average sulfur content of diesel fuel was 0.35
weight percent in 1984 and 0.03 weight percent in 1985-1986.  Other fleets analyzed
only lubricating oil.  The data showed a significant decrease in iron content in the used
oil for most engine types between the 1984 and 1985-1986 periods.  Most of the wear
reduction can  be attributed to the  lower sulfur diesel  fuel.  However,  there were
changes in the  new lubricating oils (TBN alkalinity and zinc anti-wear additive) which
could be minor contributors to the reduction in wear metal.  Some engines showed no
reduction or an increase in iron levels after the change in fuel sulfur content.
                                       Xlll

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1.    INTRODUCTION
     1.1    Background
     A study prepared for  EPA  by Energy  and Resource Consultants, Inc.  (ERC)
investigated  the effect of  diesel  fuel  sulfur content  on engine  wear.U)*   ERC
concluded that  a  reduction  of  diesel fuel sulfur  content from  0.27 to 0.05 weight
percent would result in a 30 to 40 percent reduction in engine wear and therefore a 30
to 40 percent increase  in engine life and oil drain interval.  These conclusions were
based primarily  on the  results of a study by Tennyson and Parker presented in SAE
Paper  No.  700892  (2),  which  was conducted  in a two-cycle locomotive engine.
However, today's engine oils have additive packages which are better able to handle
the corrosive wear from fuel sulfur, and some uncertainty exists in extrapolating the
locomotive engine results to on-road diesel operations.  A further investigation was
initiated into the effects of low-level diesel fuel sulfur content on engine wear.

     L2    Objective
     The objective of this work was to determine the overall magnitude of the effect
of diesel  fuel sulfur content on  the wear of heavy-duty diesel engines  in on-road
service, on  engine life, and  on oil drain intervals.  The range of fuel sulfur levels of
interest  are from 0.05 weight  percent  to current U.S. levels  (approx.  0.3 weight
percent).

     1.3    Approach
     The approach included the following work areas:
     1.     A literature review was conducted to develop an understanding of the role
            of diesel fuel sulfur  content in  the wear of  heavy-duty on-road  diesel
            engines. The effects of engine operating conditions on wear were also
            investigated, and the  effects of engine oil  additives and oil alkalinity
            (TBN) were examined.
     2.     Major U.S. diesel engine manufacturers were contacted for  their recom-
            mendations regarding operation on low and high sulfur diesel fuels.
     3.     As  an empirical check on  the literature study,  diesel fleets which  are
            currently operating on 0.05  weight percent sulfur fuel were  contacted to
            obtain used oil  analyses.  This effort  was concentrated in  the Southern
 * Underscored numbers in parentheses refer to the list of references at the end of this
 report.

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            California area,  which has undergone a legislated reduction in diesel fuel
            sulfur content to 0.05 weight percent maximum. Comparison was made of
            used oil analyses prior to sulfur reduction with those obtained after the
            reduction to determine the effect of fuel sulfur reduction on engine wear.

2.    LITERATURE REVIEW
     2.1    Introduction
     In examining the effect of  diesel fuel sulfur content on  engine wear,  it is
advantangeous to use a systems approach. Diesel engine wear is a very complex event
which includes interactions of the following system variables:

           •    fuel properties (e.g., sulfur content)
           •    lubricant properties (e.g., alkalinity content)
           •    engine design and materials
           •    engine operating conditions

     The literature search  was designed  to  obtain  information on 1) fuel sulfur
effects, 2) lubricant alkalinity effects, and 3) engine operating conditions  on high-
speed diesel engine wear. Engine design and materials considerations were beyond the
scope of this investigation and were not included in the search.

     The following five computerized data bases were searched:

           1.    SAE Global  Mobility     1968 - 1986
           2.    NTIS                    1964 - 1986
           3.    Compendex             1970 - 1986
           4.    Chemical Abstracts      1967 - 1986
           5.    DOE Energy            1974 - 1986

     In addition, SwRI files on fuel  sulfur effects were examined.  Overall, a large
body of information on  fuel sulfur  effects in high-speed diesel  engines  was found.
Several publications with data in the fuel sulfur  range  of  interest were found which
were not included in the ERC report.   In the following sections,  a  general overview of
fuel sulfur  effects on high-speed  diesel engine wear and deposits  is presented for  fuels
in the range of zero to 2 weight percent sulfur. This brief  summary documents the
fuel sulfur  content/engine wear relationship, and is followed by a  detailed discussion of

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data in the zero to 0.3 weight percent fuel sulfur range.  Detailed discussions are also
presented for the effects of operating conditions  and lubricant alkalinity (TBN) on
diesel engine wear.

     2.2.   Discussion of Literature
            2.2.1   General Diesel Fuel Sulfur Effects
     One of the early considerations of fuel sulfur  effects was presented in Ricardo's
1933 lecture in which he proposed that much cylinder wear was corrosive and related
to fuel sulfur  content.(3)  During the  1940's,  several researchers reported  on the
detrimental effects of sulfur compounds in diesel  fuel.  Cloud and Blackwood (1943)
used both cyclic and  steady-state 80-hour engine test procedures in a  Detroit Diesel
3-71, Caterpillar single-cylinder, and Hercules 6-cylinder to determine the effects of
diesel fuel sulfur content on deposits and wear.(4)  They reported that an increase in
fuel  sulfur from 0.2  to  1.0 weight percent resulted in  a two  to  sixfold increase in
measured piston ring wear, and a two to fourfold increase in cylinder bore wear.  A 40
to 80 percent increase in ring zone deposits was observed,  as well as increased ring
sticking.   Cloud  and Blackwood concluded  that   fuel  sulfur  type  was relatively
unimportant  as fuels  containing naturally occurring and added sulfur (carbon disulfide
and diamyl  trisulfide) produced about  the  same  level of engine distress.  Increased
wear and fouling  were also caused by  the addition of small amounts  of SO2 to the
intake  air of a fired engine.  Addition of SO3 to the intake air  of a motored engine
caused dramatic increases in ring wear and deposits.  Finally, they reported that 60 to
90 percent of the fuel sulfur was converted  to SO3 during the combustion process.

     In 1947, Moore  and Kent determined  the effect of  fuel sulfur content on single-
cylinder diesel engine (Caterpillar) wear by  using crankcase used oil iron content as an
indication of wear.(5) Fuels containing natural sulfur (0.7 weight percent) and sulfur
added as thiophene (0.7 weight percent sulfur) produced a four to fivefold increase in
iron  wear metals compared  to the low sulfur baseline.  A fuel with 1.3 percent sulfur
present as  thiophene gave  a  sevenfold increase  in iron wear metals.  They  also
reported that reducing engine coolant temperature  from  160°F (71°C) to 100°F (37°C)
caused a fourfold increase in wear when using fuels with no sulfur present.

     Also in 1947, Blanc of Caterpillar Tractor Co. reported that experiments in a
single-cylinder  Caterpillar engine showed that as fuel sulfur content increases, ring
and cylinder bore  wear (top) and piston deposits increase.(6) When the sulfur content

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of the fuel  is increased above 0.5 percent, the pistons become progressively dirtier,
the ring grooves pack with carbon, and the rings become more sluggish.  With  sulfur
content greater than 1.0 percent, stuck  rings become common.  Blanc reported that
distillation range of high sulfur fuels was found to affect deposits somewhat, but not
to the extent that fuel sulfur content impacted on deposits.

      In 1948, Gadebusch reported that fuel sulfur content alone is not satisfactory for
predicting engine deposits.  He found that a fuel blend of straight run and catalytically
cracked materials which contained 0.6 weight percent sulfur gave  more deposits than a
straight  run fuel with  a  sulfur  content of 1.15 weight  percent.(7)   Cattaneo  and
Starkman (1948) reported that ring wear increased threefold in going from zero  to 1.0
weight percent fuel sulfur and  that basic  material  in  the  engine oil  significantly
reduced the  wear.(8)  Furstoss (1949) investigated field  experience involving small-
bore  medium-speed diesels using high-sulfur fuel and reported that operation on fuel
with greater than 0.5 weight percent sulfur  resulted in abnormal upper  cylinder and
ring wear  with increased  engine deposits.(9)   Also  in  1949, Broeze reported that
cylinder  bore wear increased twofold and ring wear  increased  threefold  when fuel
sulfur was increased from  0.08 to 1.5 weight percent.0.0)  In experiments  with a Pyrex
window in the combustion chamber, Broeze observed that increased fuel sulfur content
caused increased lacquer deposits.

      After  the excellent research of the 1940's, very little information was published
the next 20  years  on  high-sulfur fuel usage  effects in high-speed  diesel engines.  In
1974  Perry  and Anderson  of  the U.S. Navy reported on the effects of increasing the
sulfur content of diesel fuel marine (DFM).(H.)  They found during 1000-hour tests that
in going from 1.0  to  1.3 weight percent fuel sulfur (all naturally  occurring), top
compression ring wear increased by a factor of  2.5, and more ring sticking occurred in
both two- and four-cycle diesel engines.

      U.S.  Army  research on  high-sulfur  fuel  utilization  was reported  by  Lestz,
LePera, and Bowen in 1976.(j_2)  Using a cyclic operating procedure in an aluminum
block two-cycle diesel engine, they found severe increases in fire ring (1.4  to sixfold)
and bore wear  (zero to three  fold) when comparing reference  fuel (0.4 percent sulfur)
with  fuels  containing 0.64 and  1.2 weight  percent naturally  occurring sulfur.  Higher
lubricant ash content helped in controlling fire ring and bore wear; however, more ring

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sticking occurred with the higher ash oil.  In this work, greater engine distress  was
consistently observed with the 0.64 weight percent sulfur fuel than with the 1.2 weight
percent fuel.  This  greater distress led the authors  to  speculate that other  fuel
components present such as olefinic compounds, oxygenated compounds,  naphthenic
acids, and pyrrole nitrogen were contributing to the increased wear.

     In 1978, Frame reported that in going from 0.4 to 1.0 weight  percent  naturally
occurring fuel sulfur, fire ring wear increased  fourfold and liner scuffing increased
five to tenfold in a two-cycle diesel  engine.U3)   No  change  in engine  deposits
accompanied the fuel sulfur increase in this work.

     Gergel (1980), reported on modified Cat 1-G2 tests run with fuel containing 1.4
weight percent sulfur, with the additional sulfur added  as tertiary butyl disulfide.(_14)
In these tests,  which were  run without the  standard  oil drains, piston top groove
deposit filling remained the same while weighted  total piston deposit  rating (WTD)
increased threefold; and top ring wear, as  determined by weight loss, increased
twenty-four  fold when the high  sulfur fuel was used.  Recent work on fuel sulfur
effects has been reported by McGeehan.  In 1982  McGeehan found, as Gergel  had
earlier, that fuel sulfur  content has very little effect on high temperatures (200° to
260°C) piston top  groove deposits  in  a single-cylinder  supercharged  Caterpillar
engine.(L5) In these experiments,  fuel sulfur content was increased by adding tertiary
butyl disulfide to the base fuel.  Total piston deposits increased overall with the higher
sulfur  fuel due to  increased lower  area piston  deposits at temperatures of 120  to
190°C. In 1983 McGeehan  published results of research covering the effects of  fuel
sulfur  content on diesel  engine  bore  polishing.Q6)  He found in going from 0.2 to 1.0
percent fuel sulfur, bore polishing increased two to threefold in the Mack T-6 600-hour
test, and sixfold in the 200-hour Ford Tornado test.  Finally, in 1985 Frame reported a
two to threefold increase in used oil  iron content when going from zero to 1.0 weight
percent fuel sulfur in a single-cylinder 4-cycle diesel engine operated at 180°F coolant
out temperature.(J7) In this work an unformulated lubricant was used to isolate  fuel
effects and to eliminate  acid neutralization by the lubricant.

     In summary, fuel sulfur content has been shown to be  directly  related  to engine
wear at all fuel sulfur content levels. While many factors such as operating conditions
and lubricant quality impact on engine  wear, the effect of fuel sulfur  content on

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engine wear is  great.   In general,  for  each additional  one percent of  fuel sulfur
content,  (e.g.,  0.3 to 1.3 percent  sulfur),  ring  and  cylinder  bore wear increased
approximately eightfold and fourfold, respectively.  Also, increased fuel sulfur content
generally led to additional piston deposits and often even to ring-sticking.  Most of the
above references covered fuel sulfur effects which went beyond the range of current
EPA interest. In the following section, research results in the fuel sulfur range of EPA
interest (0.05 -  0.3 weight percent sulfur) are examined in detail.  Diesel fuel sulfur
effects in the 0.05 - 0.3 weight percent range are compared with effects in  other
sulfur ranges of the same magnitude.

            2.2.2   Low-Sulfur  Diesel Fuel Effects
     The literature review revealed several  publications which contained engine wear
data in the zero to 0.3 weight percent sulfur range.  Only data which had at least one
actual data point in  the  zero to 0.3 weight percent  sulfur range  were  considered.
Extrapolations of data from  higher  sulfur  ranges were not  considered.   Each cited
result will be analyzed in terms of its applicability to current lubricants and on-road,
heavy-duty diesel engines.

     Cattaneo and Starkman (1948)  reported on  the effect of fuel  sulfur content on
measured ring weight loss, while operating at a coolant  temperature of 210°F.(8) Their
results are plotted in Figure  1, from which it was calculated that in  going  from 0.3 to
zero weight percent sulfur, ring wear (weight loss)  decreased 37 percent.  While  this
wear decease is  large on a percentage basis, the absolute ring wear rate  at 0.3 weight
percent sulfur was below 2 mg/HR.  The  Cattaneo and Starkman data did  not specify
the  engine  type,  number  of cylinders,  speed, or  load.   In addition, the type  and
properties of the lubricant used are unknown; however, at best the oil would  be 19*8
vintage, and not of the quality of current engine oils. Because of the above mentioned
unknowns, applicability of  these results to current diesel engine wear is  questionable.
It is interesting to note that  the wear curve appears to be approximately linear over
all sulfur ranges up to 1.4 weight percent  sulfur.

      Moore  and Kent (1947) conducted their  work in a single-cylinder  Caterpillar
diesel engine operating at 75 BMEP, 160°F coolant out temperature (COT), and used a
formulated, commercial heavy-duty engine oil.(5)  As shown in Figure 2, total engine
wear in mg/60 HR as determined by used oil  analyses decreased by 43 percent  in going

-------
D)
D)
    o  -
                                                                       -i	u
          0
             .5                        1
                   Fuel   S,   %
Figure 1. Effect of fuel sulfur content on piston ring wear (10)
1.5

-------
00
       L_
      o
       O)
       o
       Q)
          1200
          1000
           800
           600
 Q>
-i   400
      "D
       C
       0   200 h
       O)
       c.
              o  -
                   0
                                                                       _i	L.
                                   .5                     1
                                        Fuel  S,  %
                       Figure 2. Effect of fuel sulfur content on engine wear (5)
1.5

-------
from  0.3 to zero  weight percent fuel sulfur.  In this work, the wear rate increased
above 0.7 weight percent fuel sulfur.

      Broeze  and  Wilson  (1949),  used  a  single-cylinder Caterpillar  diesel  engine
operated at 75  BMEP, with a  COT of 140°F.UO)   Their  results show  virtually  no
difference  in  cylinder bore  wear for fuels  in the zero  to  0.5  weight percent sulfur
range as shown  in Figure  3.  Bore wear started  to  increase substantially with fuels
which contained greater than 1.0 weight percent sulfur.  While the lubricant  used in
this work was not described, the  fact  remains  that no  decrease in bore wear was
observed from 0.5 to zero weight percent fuel sulfur.
                  1
                                  Fu«) sul
                                      - i-i
                                              2-0
                                                          J
                                                         ^A
                                                    2-5     30

             Figure 3. Effect of fuel sulfur on cylinder bore wear (10)
     Malyavinskii and  Chernov  (1958), examined fuel sulfur effects  in  high-speed
Russian diesel engines, using a formulated engine oil.(18)  The engine oil  met Soviet
specification COST 5304-50.  The TBN of the new oil was not stated and  how COST
5304-50 compares to API service classifications is not known.  COT was  not stated.
As shown  in Figure 4, a reduction of fuel sulfur from  0.3 to 0.2 weight percent would
result  in  approximately a  10 percent  decrease  in relative  cylinder liner wear  as
determined by used oil analyses extrapolated to 1000 hours. Figure 5 shows results in
a different engine  using  the same oil fortified with a  supplement  anti-corrosion
additive.   In this case a  reduction  of 5 percent  in cylinder liner wear would  be
expected in going from 0.3 to 0.2 weight percent fuel sulfur.

     Pinotti, Hull, and McLaughlin (1949), conducted wear tests  in a single-cylinder
diesel  engine  operating at  175°F COT and  150°F oil sump temperature.(_19)  Top

-------
       200
   CO
        150
 0)
100
         50
o_o

   J.)
    o
   o
  0 -
                                                           -I	L
                0                     .5                      1

                                            Fuel  S,  %

                  Figure *. Effect of fuel sulfur content on cylinder liner wear with engine oil 1 U8)
                                                                            1.5

-------
 LTg
 O.E
JO) O)
    c
   LU
   CN
"So
O
        200
        150
        100
50
           0  -
                 0
                                                                                  1.5
                                               Fuel   S,  %
                        Figure 5. Effect of fuel sulfur content on cylinder liner wear, engine oil 1
                                        with anti-corrosion additive (18)

-------
compression ring wear  was monitored by using an irradiated cast-iron ring.  In going

from 0.3 to 0.05 weight percent fuel sulfur, a 15 percent reduction in ring wear was

observed (Figure 6).  While the quality of oil used in obtaining Figure 6 data was not

stated, the authors did publish results which reveal the relative ring wear performance
of 19^9 vintage engine oils:


                                  Typical Wear Rates

                                                Iron Wear Rate,
                                                  mg per hr.

                Uncompounded Oil                     1.81
                Heavy-Duty Oil Meeting Army
                   Ordnance 2-104B Spec.              1.06
                Heavy-Duty Oil Meeting Caterpillar
                   Tractor Series 2 Reqmts.            0.65


Fuel sulfur content used in obtaining these wear  rates was not specified.  The  wear

rate for uncompounded oil was  similar to  that reported  by  Cattaneo and Starkman

(Figure  1) for 0.3 weight percent fuel sulfur.(8) The ring wear reported by Pinotti, et

al., was linear over the range investigated.  (0.05 - 1.2 weight percent sulfur.)
                      100
                             Oi
                                    0.4    Oi     0«
                                      PERCENT  SULFUR
                                                        10
    Figure 6.  Relation between fuel sulfur content and ring wear, single-cylinder
       four-cycle engine, 4Jt-in. bore, 1*00 rpm.l50oF oil sump temperature.
              800 F exhaust temperature.   175HF jacket temperature.

     Mercedes-Benz Truck  Company, Inc.  has provided EPA with data on fuel  sulfur
effects  in  a draft  SAE  paper.(20) A radionuclide technique was used  to  determine

cylinder liner wear at various fuel sulfur levels and engine operating conditions.  Wear

tests were conducted in  a four-cycle, direct  injection, naturally aspirated  V-8  diesel
                                       12

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engine with one cylinder bore activated.  The engine oil met API service classification
SE/CC and was 20W-20 viscosity grade.  The oil had be to be changed frequently to
retain  resolution  of  the measuring method; thus, TBN  depletion effect could not be
investigated.  Wear  tests were conducted at fuel sulfur contents of  1.2, 0.26 and
0.05 weight percent.

     An empirical wear equation was developed and validated.  The calculated wear
rates  for  fuels in the range of zero to 0.5  weight percent sulfur are presented in
Figure 7.  These  diagrams illustrate that a reduction in fuel sulfur level  results in a
substantial reduction in engine  wear at COT below 80°C (176°F).  Reduced corrosive
wear during conditions typical of cold-start and warm-up was observed. For example,
at 50  C (122 F) COT, an 80 percent reduction in cylinder bore wear rate was observed
in going from 0.3 to 0.05  weight percent fuel sulfur. By 70°C (158°F), the reduction
                  2 10
                      20
30   AO   50  60   70  80   90 100
COOLANT OUTLET TEMPERATURE l*C1
                 Figure 7.  Wear rates with reduced sulfur content
was 28 percent  and at approximately 80°C (176°F) the observed wear rate was  the
same for 0.3 and 0.05 weight percent fuel sulfur. Beyond 80°C (176°F), at higher than
normal COT's (>80 to 85°C), fuels with very low sulfur content (0.05 weight percent)
could cause a slight increase in wear rate.  Of all the data reviewed, the Mercedes-
                                       13

-------
Benz results appear to be most directly applicable to current U.S. on-road, heavy-duty
diesel engines. Still, current diesel engine oils are of  slightly higher quality than API
classification  CC,  and  the  Mercedes-Benz experiments did not include highly  loaded
turbocharged  diesel engines.  Both  of  these factors  reduce the applicability  of  the
Mercedes-Benz data to current U.S. conditions.  In the following section, the effects
of engine operating conditions on diesel engine wear will be discussed, and the overall
importance of these effects in relation to fuel sulfur effects will be examined.

            4.2.2.3. Operating Condition Effects
     The effect of engine  operating temperature, generally expressed as coolant out
temperature (COT), on diesel  engine wear  has been extensively documented  in  the
literature.  Broeze and Wilson (10) documented an increase in piston  ring and cylinder
bore wear as  COT was lowered, using both high and low sulfur fuels (Figures 8 & 9).
                1-5 /sulphur fuel
               |X&08Z sulphur fuel
               Jesulphurlsed M^sulphurTuel)
               Wwr on 1-5/f sulphur fuel of
                  60'C taken as 100
              20   40   60   80
               Jacket outlet temp"C
                (b(TLe.p.70p.s.l.)
Figure 8.   Effect of jacket temperature
  on piston ring wear with fuels of dif-
         ferent sulfur content.
1000
1 800
>
! 900
?
!|400
!
200
n
ol-b^
x-
ii —

?
^
               Jacket outlet temp^C
                                 too
Figure 9.   Effect of jacket temperature
   on bore wear with fuels of different
             sulfur content.
The observed ring  wear increase was very slight for  0.08  weight percent fuel sulfur,
and no  bore  wear  increase  was  observed.   Blanc  (6)  conducted  single-cylinder
Caterpillar engine  tests using 1 weight percent sulfur fuel and observed the following
increase in top ring wear at lowered COT:
                 COT, °F                       175
                 Top ring gap increase, IN       0.028
                  100
                  0.045
Pinotti, et al. U9) also showed a substantial increase in iron wear rate at reduced COT
(with unknown sulfur content of the fuel):

-------
               Jacket
           Temperature,  F
    Load, %
Iron Wear Rate
   mg per hr
                 180
                 125
       100
       100
     0.48
     0.83
     Nutt,  Landen, and  Edgar  (1955), reported  on the  effect  of engine  jacket
temperature on  piston ring wear.(20  Their results, shown in Figure 10,  show wear
increasing below 150°F COT.
                Z   300
                o
                X
                «
                P '00
                ..5
                u«
                >
                ^
                2   ioo
                       75
100      129      ISO
 ' JACKET TEMPERATURE OE6  f
                                                    173
          Figure 10.  Piston-ring wear related to coolant temperature in a
                  two-stroke diesel engine (unknown fuel S level)

     Moore and Kent (1947), reported that when using 0.7 weight percent sulfur fuel
(HSF), increasing the jacket temperature from 100 to 160°F decreased engine wear by
a factor of nearly 4.5.(5) For a sulfur-free fuel (LSF), the decrease in wear going from
100 to 160°F jacket temperature was slightly less than a factor of 4 (Figure 11).  In
comparing the  actual wear rates, Moore and Kent  found the effect  of  low coolant
temperature on the rate of wear was nearly as great as increasing fuel sulfur content
by 0.7 weight percent sulfur.

     Bolis,  Johnson,  and  Daavetilla (1977)  determined  the  effect  of  COT on  top
compression ring chrome face wear rate.(22) A radioactive tracer method was used to
determine the ring wear rate of  the Cummins VT-903 engine. The results are shown in
Figure 12.  Somewhat  surprisingly,  they have shown that ring wear  increased with
increasing COT, when using fuel with 0.23 weight percent sulfur.  The authors offer
the following explanation for these results:
                                       15

-------
    1500
              —A—
    1200
O>
o
0)
c
o
     900
     600
     300
       0 h
            0
HSF, 160°F
HSF. 100°F
LSF.  160°F
LSF,  100°F
   10
20
   30
Hours
40
50
60
               Figure 11. Effect of fuel sulfur content and jacket temperature on engine wear (5)

-------
                   200 •
                 oc
                 u
                 O
                 i
                 I
                 c
                   IOO
ENGINE SPEED I8OO RPM
LOAD(BMEP) 90% FULL LOAD (117 PSD
INLET OIL TEMP. 205 f
 ~io5
                                                  ieo
                                                        200
                              OUTLET COOLANT TEMPERATURE. »F
            Figure 12.  Top compression ring chrome face wear rates for
              Cummins VT-903, 1800 rpm, 90 percent load 205^F inlet
                   oil temperature. 0.23 weight percent Fuel S.

                "The absence of corrosive wear  in  our tests  indi-
           cates that probably some variation in diesel engine design
           and/or  lubricants  has shifted  the  corrosive  wear  range
           outside our  region.  Our engine was a turbocharged, non-
           aftercooled  diesel which would  have  higher minimum
           cycle temperatures and  pressures than would a similar
           naturally aspirated diesel. Other design factors may also
           play an important  role in the negligible corrosive wear. It
           also widely  recognized that lubricants  have significantly
           improved  in their  alkalinity capacity during  the past 15
           years."

     We  believe  the  chrome ring was  impervious to corrosive  wear under  the
conditions  and  durations tested.   The Mercedes-Benz  data for a nonturbocharged
engine (Figure  7) show that for a given fuel sulfur  level, bore wear typically increases
with decreasing COT below normal operating temperature and increases with increas-
ing COT above normal operating  temperature.(20)  In general, engine wear can be
expected to increase  at COT below  the normal operating range, with the effect being
magnified by increased fuel sulfur content.
                                        17

-------
     The effect of engine load  on engine wear  has also  been documented  in the
literature.  Increased load caused increased top ring wear at various COT as reported
by Bolis, et  al., and shown in  Figure  13.(22)  The  Mercedes-Benz data (Figure  1<0
confirm the higher engine wear at increased load (BMEP and peak pressure).(20)  At
83°C COT, the  Benz data show load to be of greater importance to bore wear than
fuel  sulfur levels of 0.05 and 0.5 weight percent.  Thus, increased engine load  causes
increased engine wear rate.
                   200
                  I
                  o
                    100
                  s
                  I
2600 RPM
209 f INLET OIL TEMPERATURE
                           100
                                 120
                                       140
                                                   180
                                                         2OO
                               OUTLET COOLANT TEMPERATURE.^
                Figure 13.  Effect of load on top ring wear rate as a
                      function of outlet coolant temperature
         E
         I
         -0.3
         UJ
         IT
         cr
            0.1
                = 0.05V.wt
                = 0.50V.wt.
             "02468
                    BMEP fbarl
                     60               70
                          PEAK PRESSURE tbar)
        Figure 14. Effect of load (BMEP and peak pressure) on bore wear rate
                                        18

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               2.2.4   Lubricant Alkalinity Effects

         Lubricant alkalinity as measured by Total Base Number  (TBN) expressed as mg

   KOH/g sample  has  long been recognized as important in controlling the deleterious
   corrosive effects of diesel  fuel sulfur content.  Ellis and Edgar (1953), demonstrated
   the  reduction  of low-temperature corrosive wear by using  alkaline lube oil addi-
   tives.^)  Figure 15 illustrates the effect of lubricant alkaline content on ring wear

   for both a two-stroke and four-stroke diesel engine. Figure 16 from the work of Nutt,
.073
.090
.029
           9 3/U BORE I30F
           tt STROKE
      8 3/U BORE
      IUOF
      2 STROKE
           29       50       79       100
            OIL ADDITIVE CONTENT HIUIMOLS
   Figure 15. Low-temperature corrosive wear
   is reduced by use of alkaline lubricating
   oil additives.  These tests were of 480-hr
   duration at water jacket temperatures of
   130 and 1*0 F as noted.
                                                   10
                                                   .
                                                               too f
                                                               If SULFUR FUEL
                 2       U
             BASE  NUMBER MG KOH/G
Figure 16. Corrosive wear is re-
duced through use of alkaline oil
(indicated by base number) in a
four-stroke diesel engine at full
load with a jacket temperature of
100°F.
   et al. (1955), also shows the reduction of a low-temperature corrosive wear by using an
   alkaline oil. (
         Gergel (1980), presented  a discussion of diesel engine oil alkalinity values.(24)

   The following table lists the approximate TBN level of various diesel engine oils:
                         Diesel Engine Oil Type                 TBN

                         Universal*                            6-10
                         Generation 3 railroad                  10
                         Generation 4 Railroad                 13
                         Medium Speed Marine                 20-30
                         Cross-Head Marine                    50-70

                         *  1.000 percent total sulfated ash oil meeting
                            API CD, API SF, MIL-L-2104D, MIL-L-46152B.
                                           19

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     Gergel also presented a discussion of techniques used to measure TBN.  It was

concluded that ASTM D 664  measures protective TBN of  a used oil, while ASTM

D 2896 gives misleading higher  values because it measures  both protective TBN and

the less-protective form  of TBN which comes  from  weak nitrogen  bases (ashless

dispersants).  Figures 17 and 18 illustrate the different used oil TBN values of D 664

     Field Test Data - Caterpillar 1693 Engines
            (Fuel S nominally 0.3%)
                      ' - -. £u .
  w

•a- *

Q '
  7

Z t


Z
to «

  1

  1

  1
                                                                   • ASTM D 2896
                                                      Test Conditions
                                                         Cat  10
                                                         No Oil Drain
                                                         500  Hours
                                                         1% Sulfur Fuel
                                                                      ASTM D 664
         i u  :t  20 :•  :i
              OIL mic i :an
                        Jt  31
                                                           B    xn
                                                            Test Hours
Figure 17.  TBN/TAN versus oil miles
                                            Figure 18.  Comparison of ASTM D 664
                                               and ASTM D 2896 TBN Analyses
and D 2896. In summary, the alkalinity value (TBN) of a lubricating oil has been shown
to be  very  important in controlling  corrosive  engine wear at  low  temperature
operating conditions.  Care must be used when discussing new and used oil TBN values
because of the differing values produced by ASTM D 664 and D 2896.
            2.2.5   Fuel Lubricity Effect

     Diesel fuel sulfur content may affect fuel lubricity according to work of Wei and
Spikes.(25) A high frequency reciprocating machine was used to simulate the lubricity
of diesel fuels in fuel injection pumps.  Model sulfur compounds were added to a high-
wear severely hydrotreated fuel as shown in the following table:

            Wear Test Results Using Sulfur-Containing Model Compounds
Test Fluid

Fuel 13*
Fuel 13 + cyclopentyl sulphide
Fuel 13 + benzyl mercaptan
Fuel 13 + dibenzyl disulphide
Fuel 13 + dibenzyl disulphide
Fuel 13 + n-dodecylsulphide
                                  S from Added Compound
                                           Wt%
                                       0.01 (100 ppm)
                                           0.01
                                           0.01
                                             1
                                             1
Wear Scar Diameter
       (mm)

       0.35
       0.38
       0.40
       0.35
       0.49
       0.39
*  Fuel 13 is high wear, severely hydrotreated fuel.

                                       20

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The authors concluded that all sulfur compounds tested were pro-wear to some extent
and generally  gave increased wear at higher  concentrations.  This effect should be
further  investigated to determine if  the reduction  of diesel fuel sulfur from 0.3 to
0.05 weight percent would benefit diesel injection pump wear.

     2.3    Comments on SAE Paper 700892
     The original  work plan included a review of SAE Paper 700892 by Tennyson and
Parker (2), to determine the applicability of its results to current on-road,  heavy-duty
diesel engine  operation during this project.  After  review comments were received
from other sources, EPA requested no further review of the paper.(26)

     2.4    Engine Manufacturers
     Six major engine manufacturers  were contacted for in-house information which
they could make  available  concerning fuel sulfur effects in  the range  of  0.05 to
0.3 weight percent.  Only  two of the manufacturers were helpful; Caterpillar provided
a brochure (27) on fuel sulfur effects  and  Mercedes-Benz Truck Co. provided a  very
useful draft SAE paper (20) which was referenced in previous sections. Gergel (1980)
published the  Table  1 on engine builder  recommendations relative to  fuel sulfur
content.(24) Based on the information in  Table  1,  the  usual efforts  to control fuel
sulfur effects  are: 1) more frequent oil changes,  2) specifying new oil minimum TBN,
3) specifying a used oil minimum TBN. In conclusion, all manufacturers tend to regard
TBN depletion as an important parameter.

     The following information was obtained from  representatives of Detroit Diesel
Allison (DDA)  during a telephone conversation, and is presented with their consent.(39)
This information was received too late to  be integrated into the literature study, and
written reference  for the data has not been released by DDA.

     Engine wear studies were conducted  at three fuel  sulfur  levels (0.05, 0.26, 0.95
weight percent).   Engine  chrome ring wear was determined using a  ring irradiation
technique and measuring  wear debris  in the used oil.  Details of the wear tests are
presented in the following summary:

                      Engine type                Four-cycle turbocharged diesel
                      Operating conditions       1200 RPM max torque
                                                1800 RPM rated horsepower
                                       21

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Table  1.  Attitude of Diesel Engine Builders Relative to Sulfur
                           Content of Diesel Fuel
     Engine Builder

     Caterpillar (28)
     Cummins (29)
      Daimler-Benz (30)


      Detroit Diesel (31,32)
      Deutz (33)




      International Harvester (34)






      MACK

      M.A.N. (35)




      Mercedes-Benz (36)



      Volvo (37)
                                              Position on Diesel Fuel Sulfur Content
U.S.A.     A. Drain Interval Reduction
             96 Fuel          Drain
               Sulfur         Interval
             <0.1.0           25% Normal
          B. Standard Drain Interval
             1. For fuels up to 1.5% sulfur
             2. Oil quality
                a.  API CD
                b.  TBN - 20 times % sulfur
                c.  Unknown fuel sulfur
                   Area            TBN
                   0757A.          ~IO"
                   Canada            10
                   All others        20
             3. ASTM D 2896 for TBN
             I). Oil drain at 50% initial TBN
             5. Use wear metal analyses
                (chromium & iron) or drain
                  indication)

U.S.A.        1. Fuel sulfur is recommended not
                to exceed 1.0 mass percent
             2. Emergency specifications allow
                fuel to contain 2.0% mass sulfur.
                High TBN oils and shorter drain
                intervals to be used. No specific
                TBN or drain period specified.
             3. Oils of same TBN may not give
                same performance.

Germany        Reduce drain interval by 50% if
                fuel sulfur exceeds 0.5%.

U.S.A.        1. Use fuel below 0.5% sulfur for
                most satisfactory performance
             2. Reduce drain interval when fuel
                is above 0.5% sulfur (No details
                given).
             3. Applicable  for  two-  and  four-
                cycle
                engines.

Germany        Fuel Sulfur   Drain Interval, Km
                             CC/SE    CD/SE
                 <0.5%       10,000    15,000
                 >0.5%        5,000    10,000

U.S.A.          Drain Interval Reduction
                  Fuel         Drain
                Sulfur        Interval
                <0.5%         Normal
                0.5 - 1.0      50% Normal
                >1.0%         25% Normal

U.S.A.          No published Position

Germany        If high sulfur fuel  is used, change
                oil when TBN falls to 20% new
                oil value.
                TBN test method not specified.

Brazil         1. TBN retention  as determined by
                in-house test is important
             2. About 10 TBN minimum

Sweden       1. 0.55 maximum fuel sulfur
             2. TBN of  used oil must remain
                above 50% new oil value by
                ASTM D 2896 or not less than
                 1.0 by ASTM D 664.
                                         22

-------
                     Coolant out, °F
                     Oil type                   API CD, 15W-40, 8 TBN

DDA found a 75 percent decrease in chrome ring wear when going from 0.26 to 0.05
weight percent fuel sulfur content while operating at 184°F COT and 1200 RPM max
torque mode.  At  1800  RPM,  a  lesser wear decrease was observed, however, it  fell
within test repeatability  range.   DDA did not  feel  that  these results could  be
extrapolated to engine life at this time.

     The DDA results are somewhat  in conflict with the Mercedes-Benz data (20), in
that a substantial wear reduction  was observed while operating at normal  engine
temperature. Differences in the  M-B and DDA test parameters included:

                                              DDA              M-B
           Wear location                    ring              liner
           Turbocharged                     yes               no
           Oil quality                       CD               CC
           Oil viscosity                      15W-40           20W-20

Any or  all of the above factors could account for  the  difference in results.  This
comparison further exemplifies the  complexity of  the interrelationships of  diesel
engine wear variables.  The DDA data are most interesting and EPA should  remain
in contact with DDA to obtain any additional data which can be made available.

3.   FLEET DATA ON ENGINE OIL ANALYSES
     On January 1, 1985, the sulfur content in diesel fuel was reduced by regulation to
0.05 weight percent  maximum throughout the South Coast  Air  Basin, namely Los
Angeles, Orange, Riverside, and San Bernardino Counties in California.  This  change
provided an  opportunity to gather fleet data indicating whether or not lower sulfur
diesel fuel may result in a  reduction in engine wear and an  increase in engine life and
oil change interval. Data on diesel fuel and used engine oil analyses were sought from
fleets operating  in the area before and after sulfur content  was changed.  This  section
describes the data obtained from four  fleets, and the statistical analyses of the data.
                                       23

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     3.1    Initial Contact With Fleets
     To investigate the effects of low sulfur content in diesel fuel as it relates to
engine wear, several fleet  operators in the South Coast Air Basin area were asked to
participate in the EPA study by providing fuel and used oil analyses.  In addition, oil
analysis laboratories were contacted  to  provide  other possible data sources for the
study.   The  objectives of the  study  were explained and several requirements  were
outlined to establish whether available data could be used in the study.

     The following items were  deemed necessary for a fleet to be a candidate for the
study:

      1.     Fleets must  have  been  participating in a scheduled  used oil  analysis
            program during 1984 and 1985, i.e., before and after the effective date of
            fuel sulfur regulation on January 1, 1985.
     2.     Used  oil  analysis  data could be made available  on magnetic  tape in
            compatible format for the  computer system  at  SwRI.    Due  to  time
            constraints, it  was not  feasible to  manipulate and compare the data
            manually.

Number and Type of Contacts
     Eight bus  fleets, ten truck fleets, four municipal refuse collection truck fleets,
and seven oil analysis laboratories were contacted.  The following fleet operators were
willing to release data, and did so  in time for use in the study:

      1.     Southern California Rapid Transit District
      2.     Chandler Truck  Fleet
      3.     Suppose-U-Drive Fleet (Rental Truck Fleet)
      k.     Laidlaw School Bus Fleet

The  diesel fuel  and lubricating oil analyses for  all four fleets were performed in the
laboratories of Analysts, Inc., which provided the data used in the study.

      3.2    Southern California Rapid Transit District Fleet
      The Southern California  Rapid Transit  District  (SCRTD) is located  in Los
Angeles, California, and provides urban transit and suburban service in the county of

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Los Angeles.  It has approximately 2,500 transit buses powered by Cummins, Detroit
Diesel, and MAN engines.  SCRTD has a comprehensive and organized fuel and engine
oil monitoring program in which sampling and analyses are done on a scheduled basis.

Data Obtained
     Permission was granted by SCRTD to obtain the diesel fuel and used oil analyses
data from Analysts, Inc., an analytical laboratory with corporate headquarters located
in Rolling Hills Estate, California.  The data obtained consisted of a listing of diesel
fuel samples with sulfur content,  and magnetic  computer  tape containing used oil
analysis results for 1984, 1985, and about 10 months of 1986.

Sulfur Content Data
     There were a total of 870 diesel fuel samples analyzed for sulfur content in 1984,
1985  and  1986.   After a  thorough check,  thirty  samples were   deleted due to
duplications and other errors.  The  data  were entered into the SwRI computer system,
and statistical analyses were performed  on  191 samples  identified as tank  farm
(refinery) samples and 649 as tank trailer (delivery truck) samples.

Oil Analysis Data
     The magnetic tape with the oil  analysis data contained a total of 29,949 records
for 1984, 1985 and 1986. A sample  listing of the raw data was produced to identify the
variables in the data  base. A listing of the different engine types and frequencies of
observations for each year was produced and analyzed in order to understand the data
and delete  entries where a specific  engine  type could  not be identified.  Over 80
percent of  the  deletions  were  due  to errors in engine-type identification.    Nine
variables were selected  as most  likely to be affected by high or low sulfur content in
the fuel.   In order  to eliminate questionable data, limits were established on six
variables  where  aberrations had been  noted in  the raw data.   Observations were
deleted where any of the following conditions existed:

      1.     Zinc (Zn) was less  than 500 ppm, indicating erroneous data.
     2.     Iron (Fe), copper  (Cu), and lead (Pb) were 0 ppm simultaneously, which
            would indicate missing data.
     3.     Iron, copper, and lead were  998 ppm, indicating an erroneous reading or an
            actual reading exceeding the limits of the spectrometer.
                                       25

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Original
Records
29*0
12780
1*229
Deleted
Records
282
31*2
3717
Records
Analyzed
2658
9638
10512
     *.     Fuel dilution (FOIL) was  more than  9 volume percent.  Excessive fuel
            dilution could affect wear rate or metal analyses.
     5.     Oil miles were less than 1,000 or more than 30,000, indicating analyses on
            unused oil or possible errors in recording data.

     The following adjustments were made to the data base:
           Year
            198*
            1985
            1986
     Frequency distribution plots showing wear elements versus oil miles by engine
type and year group were developed.  No general pattern could be observed at 1-9,000,
9-15,000, 15-21,000, or 21-30,000 oil mile intervals.  Means  and standard  deviations
were calculated using the same parameters as with the frequency distribution plots.
No major differences or consistent trends  were observed with the variables selected
when compared for the same year at the various oil  mile intervals.  An example of the
data for various ranges of oil miles is given in Table  2.  Iron content in the lubricating
oil shows a consistent increase  with  oil miles for  only  the  DDV71 engine in 198*.
Other engines show upward and downward trends.  Also the trends from 198* to 1985-
86 did  not show the same  effect at different oil miles.  Based on these observations,
the oil miles data were combined into a single average for each year.  The selection of
variables to be analyzed was reduced to oil-miles, iron, and total base number (TEN).

Statistical Analysis
     The objective of  the data  analysis was to compare diesel fuel and  engine  oil
analyses, determining if significant differences occurred between 198* and 1985, and
between 198* and 1986. The method used to compare the means of the variables was
the  multiple  comparison  means test.   Specifically, 3.W. Tukey (*0) derived a test
designed for pair-wise comparisons based on the studentized range that can use equal
or unequal sample sizes.  This multiple comparison of means  test is called the Tukey
test  or the "honestly significant difference" (HSD) test.  The 95 percent  level of
confidence was chosen  for this study,  which may be stated as the  5 percent level of
significance.
                                       26

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                 Table 2. Average Iron Concentration, ppm, for
                 Southern California Rapid Transit District Fleet
Oil Miles x
1984
CUV903
DDV71
DDV92
MAN866
1985
CUV903
DDV71
DDV92
MAN866
1986
CUV093
DDV71
DDV92
MAN866
                            1-9
                                           9-15
15-21
21-30
53.5
86.0
81.7
75.0

50.7
60.8
49.4
104.4

43.7
65.7
52.2
55.5
94.3
84.3
272.0
(1 Sample)
56.7
70.8
54.2
547.3
(3 Samples)
35.0
68.0
49.1
65.1
99.8
76.5
__

72.8
53.4
—
__

65.5
51.6
__
65.3
102.2
__
__

65.8
42.2
__
__

83.4
41.2
__
                            95.9
          Fuel Sulfur Content - Table 3 shows the results of the comparison test of
          fuel sulfur content between 1984 and 1985 or 1986.  There was a 91 percent
          decrease in sulfur content in the tank farm samples while the tank trailer
          samples show a decrease of 94 percent between 1984 and 1985-1986. The
          combined pool of all samples decreased  from 0.35 weight percent sulfur in
          1984  to  0.03 weight percent in  1985, and  0.02 weight percent in 1986.
          Figures 19 and 20 illustrate the information contained in Table 3.
          Fleet  Summary  of Oil Analysis Variables  - Table  4  and Figures 21-23
          present the SCRTD fleet summary of oil-miles, iron (Fe) ppm, and total
          base  number  (TBN).  There  was  no  significant  difference in  oil-miles
          between the three years.   However, there was an average  30  percent
          reduction in the iron content between 1984 and 1985 - 1986.  There was a
          significant difference in used oil TBN of 1.4 between 1984 and 1985, and
          1.6 between  1984  and  1986.   New oil  TBN levels,  according to SCRTD
          records, were 5.4 for 1984, 7.4 for 1985, and 6.1 for 1986.  Although there
          was marked increase in the used oil TBN in 1985 and 1986, it corresponds
          with the higher TBN's  in the new oils used by SCRTD during these years
                                      27

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             Table 3. Comparison of Fuel Sulfur Content For
             Southern California Rapid Transit District Fleet
Sample
Type
Tank Farm


Tank Trailers


Combined



Year
198*
1985
1986
198*
1985
1986
198*
1985
1986

No.
*9
98
**
26
582
41
75
680
85
Sulfur, M%
Mean
0.35
0.03
0.02
0.3*
0.03
0.01
0.35
0.03
0.02
Significant
Difference*

S
S

S
S

S
S
Standard
Deviation
0.09
0.03
0.01
0.13
0.0*
0.05
0.11
0.03
0.03
 In comparison of mean  values for 1985 and 1986 with 198* at the 95 percent
 confidence level;
                   S means Significant Difference
                  NS means No Significant Difference
    A
LU
O
o
    .2
                                              TRAILER SAMPLES
                                              TANK  FARM SAMPLES
                       1984
1985
1986
          Figure 19.  SCRTD fleet, sulfur content of diesel fuel,
                        trailer and tank samples
                                  28

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      LJ
      I-
      o
      o
          .5
          .4
.3
          .2
          .1
          0
                             1984
                                1985
1986
              Figure 20.  SCRTD fleet, sulfur content of diesel fuel,
                                annual average
               Table 4. Comparison of Selected Data For Southern
                     California Rapid Transit District Fleet
Variable
Oil Miles


Iron, ppm


Total Base No.


Year
1984
1985
1986
1984
1985
1986
1984
1985
1986
No.
2658
9638
10512
2658
9638
10512
2658
9638
10512
Mean
6531.2
6734.5
6424.8
85.5
57.8
58.8
4.4
5.8
6.0
Significant
Difference*

NS
NS

S
S

S
S
Standard
Deviation
3877.1
4099.6
3859.4
53.6
49.8
44.6
1.0
0.8
0.7
*  See Table 3.
                                      29

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   9000
   7000
   5000
< 3000
Ld
   1000
    140




    120




 0. 100
 Q_



 j£  80

 Ul


     60




     40
O
o
 O
 Of
     20
                       1984
                                  1985
1986
              Figure 21.  SCRTD fleet, average oil miles
                       1984      1985      1986


      Figure 22. SCRTD fleet, average iron content of lubricating oil

-------
UJ
m  5
ui
V)
<  2
o
    1
                        1984
1985
1986
          Figure 23.  SCRTD fleet, average total base number of
                             lubricating oil

      (7.4 and 6.1).  Therefore, it is not valid to compare used oil TBN's from
      year to  year because  the  new  oil TEN  levels are different.   Another
      approach was  to  examine  the  alkalinity  depletion for each year, and
      determine if low sulfur fuel resulted in the expected increase in alkalinity
      retention.  As  shown below, no consistent trend is evident in the used oil
      alkalinity retention:
Year
1984
1985
1986
New Oil,
Typical
5.4
7.4
6.1
Used Oil,
Average
4.4
5.8
6.0
TBN
Depletion
1.0
1.6
0.1
 3.   Comparison Analyses by Engine Type - Table 5 and Figures 24-35 show the
      comparison results on the four engine types identified in the SCRTD data.
      All  engines  exhibited  increased alkalinity  levels  for  1985  and  1986;
      therefore, the observation noted for this variable in Table 4 applies.
                                   31

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Table 5.  Comparison of Selected Data for Southern California
           Rapid Transit District Fleet By Engine Type
  Variable
Year
No.
                                         Mean
CUV903 ENGINES
Oil Miles
Iron, ppm
Total Base No.
1984
1985
1986
1984
1985
1986
1984
1985
1986
87
73
15
87
73
15
87
73
15
8841.3
6284.9
6160.0
55.5
51.6
42.5
4.1
5.1
5.4
  DDV71 ENGINES

  Oil Miles



  Iron, ppm



  Total Base No.



  DDV92 ENGINES

  Oil Miles



  Iron, ppm



  Total Base No.
1984
1985
1986

1984
1985
1986

1984
1985
1986
2054
5111
4836

2054
5111
4836

2054
5111
4836
6545.7
7198.5
6888.2

  82.1
  63.6
  66.2

   4.5
   5.7
   6.0
1984
1985
1986
1984
1985
1986
1984
1985
1986
458
4387
5551
458
4387
5551
458
4387
5551
6165.3
6222.7
6070.0
82.1
50.1
51.6
4.5
6.0
6.0
MAN866 ENGINES
Oil Miles


Iron, ppm


Total Base No.



1984
1985
1986
1984
1985
1986
1984
1985
1986

59
67
110
59
67
110
59
67
110

5459.3
5332.3
3993.6
78.3
130.9
95.9
1.9
4.3
5.2
                                 Significant
                                 Difference*
                                                         NS
                                                         NS
                                     NS
                                     NS
                                                         NS
                                                          S
                                                          s
                                                         NS
                                                                    Standard
                                                                   Deviation
                                                4781.0
                                                2509.7
                                                2277.7

                                                   40.1
                                                   36.7
                                                   32.9

                                                    0.9
                                                    0.9
                                                    0.6
3915.7
4316.3
4021.7

  65.7
  44.7
  46.3

   1.0
   0.9
   0.8
                                       3567.6
                                       3803.7
                                       3697.2

                                         65.7
                                         50.7
                                         40.6

                                          1.0
                                          0.6
                                          0.5
                                                 1221.0
                                                 2641.1
                                                  563.2

                                                   51.3
                                                  153.3
                                                   79.3

                                                    1.8
                                                    1.3
                                                    1.4
  *  See Table 3.
                                   32

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V)
Ld
   9000
   7000
   5000
< 3000
Ld
    1000
                        1984
1985
1986
        Figure 24. SCRTD fleet, average oil miles (CUV903 engine)
     140
  Q.
     120
 LU
     100
      80
 8   60
 O   40
 0£


      20
                        1984
1985
1986
            Figure 25.  SCRTD fleet, average iron content of
                   lubricating oil (CUV903 engine)
                               33

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       7



       6

   QQ  3
       0
                        1984
1985
1986
         Figure 26. SCRTD fleet, average total base number of

                   lubricating oil (CUV903 engine)
   9000






   7000


LJ
-J


3 5000



o



< 3000
LJ





   1000
                        1984
1985
1986
         Figure 27. SCRTD fleet, average oil miles of lubricating

                        oil (DDV71 engine)

-------
    140
   120
 CL
 CL
    100
P  80

O
O  60
g-40
     20
      0
                       1984
1985
1986
         Figure 28. SCRTD fleet, average iron content of lubricating
                          oil (DDV71 engine)
  CD
      0
                                    II
                       1984
1985
1986
      Figure 29. SCRTD fleet, average total base number of lubricating
                          oil (DDV71 engine)
                                 35

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CO
   9000
   7000
   5000
< 3000
bJ
    1000
                        1984       1985       1986


         Figure 3Q. SCRTD fleet, average oil miles (DDV92 engine)
     140
     120

  E
  Q.
  0-  100
 Ul
      80
 8   60
 O   40
 Q£


      20
                        1984
1985
1986
       Figure 31. SCRTD fleet, average iron content of lubricating
                         oil (DDV92 engine)
                               36

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   OS
   Ul
   m
   Ul
   (SI

   m  3



   2  2
   o
   I—

       1
                                 wwwk
                       1984
1985
1986
    Figure 32.  SCRTD fleet, average total base number of lubricating
                        oil (DDV92 engine)
Ld
   9000
   7000
   5000
< 3000
LJ
   1000
                       1984       1985       1986

       Figure 33. SCRTD fleet, average oil miles (MAN866 engine)
                              37

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    140


    120
Ld
o
     80
     60
     40
     20
                       1984
1985
1986
       Figure 34. SCRTD fleet, average iron content of lubricating
                         oil (MAN866 engine)
  OH
  Ld
  m
      0
                       1984
1985
1986
          Figure 35.  SCRTD fleet, average total base number of
                    lubricating oil (MAN866 engine)
                                38

-------
     a.  CUV903 Engines - There was a 30 percent decrease (significant) in the
        oil  mile  averages between 1984 and  1985,  1986.   Correspondingly,
        although not statistically significant, the iron ppm decreased from 56
        ppm in 1984 to 52 ppm in 1985 and 43 ppm in 1986.
     b.  DDV71  Engines -  Here  we  see a  significant  increase  in  oil-miles
        between  1984 and 1985, 1986.   The  iron ppm;  however,  decreased
        significantly by  20 percent; therefore,  the decrease in engine wear as
        indicated by used oil iron content could be attributed to the low sulfur
        content in the fuel.
     c.  DDV92 Engines  -  There was no  significant difference in  the oil-mile
        mean for  the three year period, however, the iron content  exhibits a
        sharp decrease from  82 ppm  in  1984 to 50 ppm in 1985, 1986.  This
        translates to a 38 percent difference.   The  low sulfur content in the
        fuel appears to have contributed to this  reduction.
     d.  MAN866 Engines - There was no significant difference in  the oil-miles
        between 1984 and 1985; however, there was a  27 percent decrease
        between 1985 and 1986.  It would be expected that the iron ppm would
        decrease relative to the oil miles; instead, there is a sharp increase of
        45  percent  between  1984 and  1985,  1986.  It should  be noted that
        samples for these engines were  less  than  1 percent of  the  total data
        base.  Very few  engines contributed  data; therefore,  if one or  two
        engines in the group were behaving aberrantly, the analysis as a whole
        would  be affected.  The very large standard deviation  for the  iron
        content as shown in Table 5 supports this observation.

3.3   Chandler, Suppose-U-Drive (Rental Trucks) and Laidlaw School Bus Fleets

1.     The Chandler  Palos  Verdes Sand & Gravel Company is located in Lomita,
      California. The fleet consists of 55 gravel trucks powered  by Caterpillar,
      Cummins, Detroit Diesel and Mack engines, and is on a scheduled used oil
      analysis program.  The fleet operates exclusively in the basin  area.

2.     Suppose-U-Drive Truck  Rental  Company is located in Glendale, Cali-
      fornia. There are  152 diesel powered rental trucks of different configura-
      tions  and  sizes.  The  principal engine  types  identified  are  Cummins,
      Detroit Diesel, Duetz, CMC, and International Harvester.  The fleet, for
                                  39

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           the most part, operates in the basin area; however, there are a few rental
           trucks that are used out of the area.

     3.    The Laidlaw  Transit, Inc. with  locations in  Los Angeles,  Van Nuys, 29
           Palms, and Palm Springs, California, operates  and maintains a total of 190
           school buses powered by  Cummins and Detroit Diesel engines. Only the
           vehicles operated  in the Los Angeles and Van Nuys area were considered
           for the study.

Data Obtained
     The  data  on  these fleets,  provided by  Analysts, Inc. laboratory, consisted of a
magnetic  tape  containing  used  oil analysis  for  198*,  1985, and 1986.  Fuel sulfur
content analyses were not available for any  of the fleets. Therefore, it was assumed
that these fleets experienced a decrease in fuel sulfur content to 0.05 weight  percent
max in 1985.

Oil Analyses Data
     The  magnetic tape contained a total of 2,152 records.  The data were separated
by fleets and listings produced to identify the variables in  the data base. It was found
that TBN  data  were not reported for  any of  the fleets. Oil mile entries were missing
from the Laidlaw fleet; therefore, the oil mile variable was not used for  comparison on
this fleet.  The data were prepared for analyses in the same manner as the SCRTD
data.  The variable zinc (Zn) was selected for comparison  due to a noticeable increase
between 198* and 1985,  1986 in the Chandler  and Rental Truck Fleet.

Statistical Analysis
     The  objectives and methods employed  were the same  as for the SCRTD fleet.
Data  on  fuel  sulfur  content were not available for these fleets;  therefore, the
assumption was made that based on geographic location, sulfur content change was
similar to that observed by SCRTD.

      1.     Chandler Fleet Summary of Oil  Analysis Variables - Table 6,  Figures 36-
            38, present the summary of oil  miles, iron (Fe)  ppm, and zinc (Zn) ppm.
            There was no significant difference in the average oil miles between 198*
            and 1985, 1986. Iron content decreased from  50 ppm in  198* to *9 ppm in
                                       *0

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                    Table 6. Comparison oi Selected Data
                         for Chandler Truck Fleet

Variable
Oil Miles


Iron, ppm


Zinc, ppm



Year
1984
1985
1986
198*
1985
1986
198*
1985
1986

No.
33
275
455
33
275
455
33
275
455

Mean
3993.9
3775.6
3*12.0
50.1
48.6
44.7
1183.0
1818.6
1940.6
Significant
Difference*

NS
NS

NS
NS

S
s
Standard
Deviation
2721.2
2734.5
3112.7
30.8
48.6
43.4
217.7
221.4
161.8
*  See Table 3.
       6000
       5000
   UJ  4000
       3000
   <  2000
   UJ
       1000
          0
                            1984
1985
1986
                Figure 36. Chandler truck fleet, average oil miles
                                    41

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      80
   Q. 60
   Q.
  Ul
  I-

  O
  o
40
       0
                        1984
                             1985
1986
        Figure 37. Chandler truck fleet, average iron content of
                         lubricating oil
E
Q.
Q.
Z
UJ
   2400
   2000
   1600
   1200
O
o
0  800
z
M
    400
       0

                                      mm.
                       1984
                            1985
1986
        Figure 38. Chandler truck fleet, average zinc content of
                         lubricating oil

-------
      1985 and finally to 45 ppm in 1986.  However, these differences were not
      statistically significant.  It is noteworthy to mention that the new oil zinc
      content was significantly different (59 percent higher) between 1984 and
      1985, 1986.  This indicates that different engine oils were used  in  1984
      and 1985-1986.  The increase in zinc content was found to be consistent in
      all of the analyses.  Therefore, because of the anti-wear properties of
      zinc oil additives, any reduction in used oil iron content could be caused in
      part by the increase in lubricant zinc level.(41)

2.    Comparison Analysis by  Engine Type - Table 7, Figures  39  through 50
      present the comparison analyses for the different engine types powering
      the Chandler truck fleet.  The 1984 data were not available for the Mack
      engines. Means and standard deviations are included for 1985 and 1986.
      a.    Caterpillar Engine - There was a significant difference in the mean
            oil miles between  1984 and 1985-1986.  The iron content for  1985
            and 1986 decreased by 11 percent, an expected occurrence but not
            relative to the 54 percent decrease in oil-miles.  The small sample
            size for  1985 possibly played a part in the results.
       b.   Cummins  Engine -  There  was  no   significant  difference  in the
            average oil-mile variable for 1984, 1985, and 1986; however, used oil
            iron content increased by 97 percent. It appears that the compari-
            son was  biased by the sample size for  1984.
      c.    Detroit  Diesel Engines -  There  was  no statistical difference in the
            oil-miles mean or the used oil iron content between the three years.
            There was, however,  a  significant  increase  in oil zinc  content
            between 1984 and  1985-1986.  The increase in zinc could result in
            less used oil iron content.  Overall the expected decrease in used oil
            iron content was not observed.
      d.    Mack Engines - No data were available for 1984  for comparison to
            be made;  however, there was a proportionate  decrease in  the oil-
            mile mean and the average iron ppm between 1985 and 1986.

3.    Rental Truck Fleet Summary of Oil Analysis Variables - Table 8, Figures
      51 through 54  present the  results of 1984,  1985 and  1986  comparison
      analyses of used oil variable means. There  were no significant differences
                                  43

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           Table 7. Comparison of Selected Data for
              Chandler Truck Fleet by Engine Type
                                                     Significant     Standard
  Variable         Year      No.        Mean       Difference*    Deviation
CATERPILLAR ENGINES
Oil Miles
Iron, ppm
Zinc, ppm
CUMMINS ENGINES
Oil Miles
Iron, ppm
Zinc, ppm
198* 6
1985 5*
1986 82
1984 6
1985 54
1986 82
1984 6
1985 54
1986 82
1984 5
1985 74
1986 138
1984 5
1985 74
1986 138
1984 5
1985 74
1986 138
DETROIT DIESEL ENGINES
Oil Miles
Iron, ppm
Zinc, ppm
MACK ENGINES
Oil Miles
Iron, ppm
Zinc, ppm
1984 22
1985 119
1986 185
1984 22
1985 119
1986 185
1984 22
1985 119
1986 185
1984 0
1985 28
1986 50
1984 0
1985 28
1986 50
1984 0
1985 28
1986 50
                                        2966.6                       1069.1
                                        1671.9            S          1285.9
                                        1038.6            S           943.4

                                          72.9                         24.9
                                          78.2           NS           70.4
                                          50.4           NS           38.5

                                        1160.0                        207.6
                                        1794.8            S           237.1
                                        1919.7            S           158.1
                                        5160.0                       1424.0
                                        4584.1           NS         2603.0
                                        4404.3           NS         3202.4

                                           9.8                           3.4
                                          17.2           NS             7.6
                                          21.6            S             14.5

                                        1240.0                         191.1
                                        1808.2            S            176.0
                                        1923.1            S            185.4
                                        4009.0                       3162.2
                                        4589.9           NS         2921.8
                                        4251.8           NS         3262.9

                                          53.2                         27.6
                                          55.5           NS           44.7
                                          62.3           NS           54.8

                                        1176.3                        232.4
                                        1829.9            S           245.9
                                        1957.4            S           147.5
                                          0                            0
                                        2235.7                        991.8
                                        1458.0                        749.9

                                          0                            0
                                          45.2                          26.8
                                          34.4                          19.3

                                          0                            0
                                        1844.2                        191.3
                                        1960.8                        143.2
» See Table 3.

-------
    6000
    5000
in
LJ 4000
-J 3000

o



< 2000
LJ
2


   1000




       0
      80
  E
  9-
  Q.
  Ld
  I-

  o
  o
40
  §  20
                         1984
                               1985
1986
             Figure 39. Chandler truck fleet, average oil miles

                          (Caterpillar engine)
                         1984
                               1985
1986
          Figure 40. Chandler truck fleet, average iron content of

                    lubricating oil (Caterpillar engine)

-------
   2400
 - 2000


 0.

 Q.

  « 1600
UJ
I—

o
o

o


M
1200
 800
     400
                        1984
                                1985
1986
         Figure 41. Chandler truck fleet, average zinc content of

                   lubricating oil (Caterpillar engine)
   6000
   5000
UJ 4000
   3000
< 2000

LJ
    1000
       0
                        1984
                                1985
1986
            Figure 42.  Chandler truck fleet, average oil miles

                          (Cummins engine)

-------
      80
   g- 60
  UJ
  I-

  o
  o
40
  §  20
       0
                         1984
                               1985
1986
          Figure 43. Chandler truck fleet, average iron content of
                     lubricating oil (Cummins engine)
    2400
P  2000

Q.
Q.
  „  1600
LJ
O
O
    1200
     800
     400
       0
                         1984
                               1985
1986
    Figure
                    Chandler truck fleet, average zinc content of
                     lubricating oil (Cummins engine)

-------
    6000
   5000
   4000
   3000
< 2000
UJ
    1000
       0
      80
   E
   Q. 60
   0.
  LJ
  I—
  z
  o
  o
40
  g  20
       0
                         1984
                               1985
1986
             Figure 45. Chandler truck fleet, average oil miles

                        (Detroit Diesel engine)
                         1984
                               1985
1986
          Figure 46. Chandler truck fleet, average iron content of

                  lubricating oil (Detroit Diesel engine)

-------
 E
 Q.
 Q.
Ld
O
o
z
N
    2400
    2000
    1600
    1200
     800
     400
       0
w,.
W
                        1984
  1985
1986
          Figure *7. Chandler truck fleet, average zinc content of

                  lubricating oil (Detroit Diesel engine)
    6000
   5000
    4000
    3000
<  2000
    1000
       0
                         1984       1985       1986


      Figure 48. Chandler truck fleet, average oil miles (Mack engine)

-------
      80
   g- 60
      40
  O
  o
  §  20
       0
                         1984
                                 1985
1986
         Figure 49. Chandler truck fleet, average iron content of

                     lubricating oil (Mack engine)
 E
 Q.
 CL
LJ
I—
z
o
o

o

M
    2400
    2000
    1600
1200
 800
     400
       0
                         1984
                                 1985
1986
        Figure 50. Chandler truck fleet, average zinc content of

                     lubricating oil (Mack engine)
                                50

-------
                   Table 8. Comparison of Selected Data
                         for Rental Truck Fleet

Variable
Oil Miles


Iron, ppm


Zinc, ppm



Year
1984
1985
1986
1984
1985
1986
1984
1985
1986

No.
264
329
384
264
329
384
264
329
384

Mean
7808.0
7514.6
8307.8
74.4
57.3
53.7
1410.9
1674.1
1818.4
Significant
Difference*

NS
NS

S
S

S
S
Standard
Deviation
3019.5
3036.4
3591.5
44.7
31.2
38.1
299.2
263.8
290.6
* See Table 3.
     V)
     UJ
        9000
        7000
        5000
     <  3000
     UJ
        1000
                          w.
m
           W,
                            1984
  1985
1986
               Figure 51. Rental truck fleet, average oil miles
                                 51

-------
  E
  a
     140
     120
     100
 LU   80
 I-

 O
 0
       60
 O   40
 oc
       20
        0
                         1984
1985
1986
          Figure 52. Rental truck fleet, average iron content of
                           lubricating oil
    2400
 c  2000

 Q.
 Q.

 »  1600
    1200
O
O
O   800
z
M

     400



        0
                         1984
1985
1986
          Figure 53. Rental truck fleet, average zinc content of
                           lubricating oil
                                52

-------
UJ
<
LJ
1.3E04

1.1 E04

  9000

  7000

  5000

  3000

  1000
                            1984
                                     1985
1986
      Figure 54.  Rental truck fleet, average oil miles (Cummins engine)

         between  the  oil-miles for 198*  and 1985-1986.  There can be  seen,
         however, a significant decrease of iron ppm.  Normally the iron  content
         would be expected to remain relatively constant given the closeness in the
         oil-mile means.  Instead, we see a 25 percent decrease  between 198* and
         1985-1986. The increase in zinc content from the anti-wear additive may
         have had a minor effect on the iron reduction;  however, the low sulfur
         fuel  appears  to  have significantly contributed  to  the  decrease  in  iron
         content.

         Comparison Analyses  by Engine Type - Table 9, Figures 55 through 71,
         show the comparison analyses for the engine  groups in  the Rental truck
         fleet.  The zinc variable shows an increase of approximately 25  percent
         thoughout the engine groups.  Due to the anti-wear properties of  zinc oil
         additives, it can be reasoned that zinc may  have had an effect in the
         reduction of iron ppm in addition to the low sulfur fuel.(*l)
                                    53

-------
     Table 9.  Comparison of Selected Data for
          Rental Truck Fleet by Engine Type
                          No.
                                     Mean
CUMMINS ENGINES
Oil Miles
Iron, ppm
Zinc, ppm
DETROIT DIESEL
Oil Miles
Iron, ppm
Zinc, ppm
DUETZ ENGINES
Oil Miles
Iron, ppm
Zinc, ppm
CMC ENGINES
Oil Miles
Iron, ppm
Zinc, ppm
INTERNATIONAL
Oil Miles
Iron, ppm
Zinc, ppm
1984
1985
1986
1984
1985
1986
1984
1985
1986
ENGINES
1984
1985
1986
1984
1985
1986
1984
1985
1986
1984
1985
1986
1984
1985
1986
1984
1985
1986

1984
1985
1986
1984
1985
1986
1984
1985
1986
HARVESTER
1984
1985
1986
1984
1985
1986
1984
1985
1986
38
34
51
38
34
51
38
34
51
126
162
200
126
162
200
126
162
200
8
16
20
8
16
20
8
16
20

2
2
4
2
2
4
2
2
4
ENGINES
90
114
108
90
114
108
90
114
108
11110.3
11769.4
13235.8
34.8
32.5
37.3
1347.3
1567.6
1806.4
7973.0
7602.3
8408.5
85.3
62.9
56.4
1363.9
1653.6
1756.4
7633.7
8462.0
7494.0
128.3
82.3
102.1
1932.5
1948.1
2217.7

7038.5
6994.5
5777.5
31.0
18.0
8.7
1115.0
1615.0
1635.0
6211.7
5982.4
5978.7
72.0
53.8
49.3
1463.8
1700.1
1862.2
                                                Significant
                                                Difference*
                                                   NS
                                                    S
                                                   NS
                                                   NS
                                                   NS
                                                   NS
                                                    NS
                                                    NS
                                                    NS
                                                    NS
                                                    NS
                                                    NS
                                                    NS
                                                    NS
                                                    NS
                                                    S
                                                    NS
                                                    NS
Standard
Deviation
 3194.4
 3199.2
 4314.5

   18.3
   18.0
   21.1

  257.9
  204.8
  152.7
 2753.9
 2565.7
 2711.5

   47.7
   33.2
   24.2

  274.5
  302.6
  299.7
  1507.2
  4196.0
  3634.0

    35.0
    30.9
   120.3

   603.4
   245.6
   473.1
   126.5
   747.4
   865.7

     2.8
     8.4
     2.7

    77.8
   134.3
    49.3
  2140.8
  2018.5
  2003.4

    36.4
    26.1
    25.8

   261.4
   186.9
   185.7
* See Table

-------
  E
  a.
  a.
140



120



100



 80
  8   60

      40
      20
        0
                         1984
                               1985
1986
          Figure 55. Rental truck fleet, average iron content of
                    lubricating oil (Cummins engine)
 E
 Q.
 Q.
Ul
O
O
    2400
    2000
    1600
    1200
O   800
z
N

     400



        0
                         1984
                               1985
1986
          Figure 56. Rental truck fleet, average zinc content of
                    lubricating oil (Cummins engine)
                                 55

-------
   9000
   7000
   5000
< 3000
Ld
    1000
                         1984
                                1985
1986
             Figure 57. Rental truck fleet, average oil miles
                        (Detroit Diesel engine)
     140
  Q.
 o
120



100



 80



 60
 O  40
 Of
     20
                      w.
                        1984
                               1985
1986
          Figure 58. Rental truck fleet, average iron content of
                  lubricating oil (Detroit Diesel engine)

-------
E
Q.
Q.
LJ
l-
Z
o
o
    2400
2000
     1600
1200
O    800


M

      400




        0
 LJ
    9000
    7000
    5000
 < 3000
 LJ
     1000
                         1984
                                1985
1986
            Figure 59. Rental truck fleet, average zinc content of
                   lubricating oil (Detroit Diesel engine)
                   w.
                         1984
                                1985
1986
              Figure 60. Rental truck fleet, average oil miles
                            (Deutz engine)
                                  57

-------
    140



    120



  -  100
 •>


S   80
   Q.
  o
       60
  O   40
       20
                          1984
                                   1985
1986
           Figure 61. Rental truck fleet, average iron content of
                      lubricating oil (Deutz engine)
     2400
     2000
 Q.
 Q.
!_•   1600


Ul
     1200
O
o
O    800

M

      400
                          1984
                                    1985
1986
           Figure 62. Rental truck fleet, average zinc content of
                      lubricating oil (Deutz engine)

-------
   9000
   7000
   5000
< 3000
ui
    1000
m
                        1984
  1985
1986
       Figure 63. Rental truck fleet, average oil miles (CMC engine)
    140
  E
  Q.
  Q.
    120
    100
 UI   80
 h-

 o
 o
      60
 O   40
      20



       0
                        1984
  1985
1986
           Figure 64. Rental truck fleet, average iron content of
                      lubricating oil (CMC engine)
                                 59

-------
 E
 Q.
 0.
o
o
N
    2400
    2000
    1600
    1200
     800
     400
                         1984
1985
1986
           Figure 65. Rental truck fleet, average zinc content of

                      lubricating oil (CMC engine)
    9000
    7000
    5000
<  3000

UJ
    1000
                         1984
1985
1986
             Figure 66. Rental truck fleet, average oil miles

                       (Inter-Harvester engine)
                                 60

-------
      140
    E
    Q.
      120
    °-100
     •t
   I-

   Uj  80
   O
       60
   O  40
       20
bJ
h-
Z
O
O
                          1984
                                1985
1986
          Figure 67. Rental truck fleet, average iron content of
                 lubricating oil (Inter-Harvester engine)
     2400
 E   2000
 0.
 CL
     1600
1200
_*    800

N

      400



        0
                              m,
                          1984
                                1985
1986
          Figure 68.  Rental truck fleet, average zinc content of
                 lubricating oil (Inter-Harvester engine)
                                61

-------
   9000
   7000
   5000
< 3000
UJ
    1000
   E
   a.
140



120



100
  UJ  80
  I-
  O
      60
  O  40
  CK
      20
       0
                         1984
                                1985
1986
               Figure 69.  Rental truck fleet, average oil miles
                           (Caterpillar engine)
                         1984
                                1985
1986
            Figure 70. Rental truck fleet, average iron content of
                    lubricating oil (Caterpillar engine)
                                  62

-------
     2400

g   2000
Q.
Q.
^  1600
UJ
     1200
O
o
O    800
z
M
      400
                            1984
1985
1986
           Figure 71. Rental truck fleet, average zinc content of
                    lubricating oil (Caterpillar engine)
             Cummins Engines - There was a slight (nonsignificant) increase in
             oil-miles between 1984 and 1985. There was, however, a significant
             increase in  oil-miles  in 1986.   The  used oil  iron  content  was
             statistically  the same for all three  years.    The iron content
             increased from  33  ppm in 1985 to  37 ppm  in 1986. This coincides
             with the 12 percent increase in oil-miles for the  same period.  The
             level of zinc increased by 25 percent between  1984 and 1985-1986,
             which could  be  impacting the  wear.  For  1986, the increased oil
             miles would be expected to increase used oil iron content, while low
             sulfur fuel and  higher  oil  zinc  content  would be  expected  to
             decrease iron. Overall, no clear effect could be determined.
             Detroit Diesel Engines - There was no significant difference in oil-
             mile means between 1984, 1985, and  1986. Iron content was reduced
             from 85 ppm in  1984 to 63 in 1985 to 56 in 1986.  The increase in oil
             zinc concentration  may account in part for the  30 percent reduction
                                   63

-------
                 in  iron wear.  Low sulfur fuel appears to have had a considerable
                 effect in reducing iron wear.
           c.    Deutz Engines - There were no statistically significant differences
                 in the three variables (oil-miles, iron, zinc) of concern.
           d.    CMC Engines - The oil-mile means were not significantly different.
                 The iron  content shows a 56 percent reduction, while the zinc level
                 increased by  *5 percent.   The  very  small  number  of  samples
                 probably invalidates the comparison results.
           e.    International Harvester Engines - Although  not statistically signifi-
                 cantly, there was a  * percent  decrease in  oil-mile  means  between
                 198* and 1985-1986.  For the same period,  iron content shows a 28
                 percent decrease from 72 ppm  in 198*  to 5* in  1985 to *9  in 1986.
                 The  sample sizes were  approximately even for the  three  years
                 compared.  Although part of the reduction in iron concentration can
                 be attributed to the 22 percent increase in zinc content, low sulfur
                 fuel appears to be related to the decrease.
     5.    Laidlaw School Bus Fleet Summary of Oil Analyses - Table 10, and Figures
           72 through 77 present the  fleet summary and engine group analyses.   The
           Laidlaw fleet  did not report oil-mile readings with the data;  therefore,
           averages were not calculated.  Due to the  relationship between oil-miles
           and iron wear, it was not possible to make an assessment of the results.
           The data are included as a matter of  information.

*.   CONCLUSIONS AND RECOMMENDATIONS
     *.l   Conclusions From Literature Review
     Throughout the literature, fuel  sulfur content has been related to corrosive
diesel engine wear.  A summary of the effects of decreasing the fuel sulfur content
from 0.3 to 0.05 weight percent is presented  in Table 11.  The data from  Mercedes-
Benz (20) are the most relevant to current lubricants  and engines.  Extrapolation of
earlier results (8, K), _18, 19) would seem  to  be  tenuous  because  they were  obtained
with older oil  formulations quite  different from the improved lubricants  which are
available today.  The results presented in Table 11 are conflicting.  Broeze and Wilson
(10) found no reduction in wear below 0.5 weight percent sulfur, even though they were
operating at  a relatively cool jacket temperature of 1*0°F and using a lower quality
19*9 vintage lubricant.   M-B found  great reductions in wear  for  low sulfur  fuels

-------
                  Table 10. Comparison of Selected Data For
                     Laidlaw School Bus Fleet (Total Fleet)
Variable
Oil Miles
Iron
Zinc
CUMMINS ENGINES
Year
1984
1985
1986
1984
1985
1986
1984
1985
1986
No.
58
92
123
58
92
123
58
92
123
Mean
DATA
31.8
27.3
49.5
1367.2
1349.1
1350.3
Significant
Difference*
NOT
NS
S
NS
NS
Standard
Deviation
AVAILABLE
20.2
17.3
57.9
109.7
113.2
78.8
Oil Miles


Iron


Zinc


1984
1985
1986
1984
1985
1986
1984
1985
1986
25
45
60
25
45
60
25
45
60
DATA


32.9
25.4
41.4
1382.0
1332.0
1345.8
DETROIT DIESEL ENGINES
Oil Miles


Iron


Zinc


1984
1985
1986
1984
1985
1986
1984
1985
1986
33
47
63
33
47
63
33
47
63
DATA


31.0
29.1
57.4
1356.0
1364.8
1354.6
                                                       NOT
                                                        NS
                                                         S
                                                        NS
                                                        NS
AVAILABLE

    20.6
    19.1
    30.4

   120.1
   109.2
    80.3
                                                       NOT
                                                        NS
                                                         S
                                                        NS
                                                        NS
AVAILABLE

    20.2
    15.3
    74.7

   101.7
   115.8
    77.7
 *  See Table 3.
                                     65

-------
       60
       50
     a
     a
UJ
I-
O
o
       30
       20
    O
    Of
Q.
Q.
O
O
       10
                          1984
                                  1985
1986
         Figure 72. Laidlaw school bus fleet, average iron content of
                            lubricating oil
     2400
     2000
     1600
     1200
O    800
      400
         0
                          1984
                                  1985
1986
         Figure 73. Laidlaw school bus fleet, average zinc content of
                            lubricating oil
                                  66

-------
        60
        50
    Q.
    Q.
    l-T  40

    LJ
    o
    o
Q.
Q.
O
o
        30
        20
        10
                           1984
                                      1985
1986
          Figure 74. Laidlaw school bus fleet, average iron content of
                      lubricating oil (Cummins engine)
     2400


     2000


     1600


     1200
O    800
z
M
      400
                           1984
                                      1985
1986
         Figure 75. Laidlaw school bus fleet, average zinc content of
                     lubricating oil (Cummins engine)
                                  67

-------
       60
   £  50

   Q.
   Q.

   . -  40
  O
  o
       30
       20
       10
        0
                          1984
1985
1986
        Figure 76. Laidlaw school bus fleet, average iron content of
                  lubricating oil (Detroit Diesel engine)
     2400



 £j   2000
 Q.
 Q.

^  1600

Ul
     1200
O
O
O    800

M

      400
                          1984
1985
1986
        Figure 77. Laidlaw school bus fleet, average zinc content of
                  lubricating oil (Detroit Diesel engine)
                                 68

-------
                                         Table 11.  Summary of Fuel Sulfur Effects
Reference

Number
Fuel S Reduction
(Moore &
Kent)
5

(Cattano &
Starkman)
8

(Broeze & Wilson) (Malyavinski &.
Chernov)
10 IS

(Pinotti, Hull,
McLaughlin)
19

(Rosow M-B)

20

(0.3 to 0.05 weight percent) Effects
COT, °F
Wear
Bore wear Reduction

Ring Wear Reduction


Total Engine Wear Reduction
Comments on Applicability to
Engines and Lubricants
Limitations



160

X

X


43%
Current

1947, HD
Commercial
oil

210

X

37%
(1.2 mg/HR
@ 0.05% S)
X


Unknown Lube
1948 vintage


140 NS*

None 10%
(0.3 to 0.2%S)
X X


X X


Unknown Lube Formulated Oil
1949 1958 Russian
Engines

175

X

15%


X


1949 Oil
Formulation


122/158/176

80%/28%/0

X


X


SE/CC Oil
Non-turbo-
charged
Engines
*  Not Stated.

-------
operating below 175°F COT.  The Mercedes-Benz data and others reveal the extreme
importance of operating temperature (COT), when examining fuel sulfur effects.  The
amount of benefit from wear reduction when operating on fuels  with  0.05 weight
percent sulfur would appear to be directly related to the accumulated amount of time
the engine operated at COT below 175°F.  This time would vary depending on the type
of duty cycle involved.  For example, on-road line haul diesel engines experience less
accumulated cold start and warmup time than engines used for in-city delivery service
with frequent stops.  Mercedes-Benz data also indicate  a possible wear increase for
low  sulfur fuels at higher than normal COT.   Overall, a single  figure cannot  be
extrapolated from the literature for reduction of engine  wear when  operating on 0.05
weight  percent  sulfur diesel fuel, due  to  the  strong temperature dependence of  the
engine  wear/fuel sulfur relationships.  Other  factors and effects such as TBN  and
engine load also have important impact on the wear/fuel sulfur relationships.

     Other  effects investigated were oil alkalinity (TBN) level and engine  load.  Oil
TBN level is very important in controlling corrosive engine  wear.  Operation on 0.05
weight  percent  sulfur fuel could allow longer  oil drain  intervals because of  reduced
TBN depletion.  No data were found which could be used to extrapolate and quantify
the expected increase oil of alkalinity retention when using 0.05 weight percent sulfur
fuel.

     As engine load increases,  engine  wear  can be expected to increase as shown in
Figure 1M20)  At the normal operating temperature point (175° - 180°F) where there
was no  effect of fuel sulfur content on  wear, (according  to Mercedes-Benz)  the effect
of engine load on wear was fairly substantial.

     Overall, operating temperature, load,  and  fuel  sulfur  content appear to be of
equal importance when discussing diesel engine wear. The complexity and interrela-
tionship of  fuel sulfur content,  operating  temperature, engine load and  lubricant
alkalinity on diesel engine wear prevent making  simple  generalizations regarding the
effects of any one of these variables.  Care must also be used in extrapolating changes
in used oil iron content, measured ring wear, and/or cylinder wear to expected engine
life. As stated  in API comments to EPA (38), the primary reasons for engine overhaul
when using today's commercial diesel fuel (0.3 weight percent sulfur average) are:
                                       70

-------
     •     Loss of oil control because of
           -   bore polishing resulting from excessive top land piston deposits which
              remove lubrication from the cylinder walls
           -   piston ring scuffing resulting from over-fueling, overheating or lack of
              oil
           -   broken piston rings  resulting from  deformation  of  aluminum piston
              grooves or overuse of Jacobs brakes
     •     Mechanical failures
           -   bearing failures due to fatigue or oil contamination
           -   camshaft failures due to manufacturing quality control problems
           -   injector failures causing over-fueling, piston burning, and/or ring scuff-
              ing

     These reasons for engine rebuild do not appear to be directly related to corrosive
ring and liner wear.

     The following is quoted from the API comments:

           "Information  available  in the literature  (SAE  Papers  Nos.
           831721 and 821216), indicates that it  is not piston ring or liner
           wear  that determines  when engines are overhauled, but  a
           variety  of other problems.   The  most  important  of  these
           problems  is loss of oil  control,  as indicated by the  MVMA
           survey.   This loss of oil control is generally caused by bore
           polishing,  ring scuffing, or broken rings.  Bore polishing occurs
           when  excessive  deposits of hard carbonaceous material in the
           top ring land abrasively  remove the the Crosshatch pattern on
           the liner.    Piston  ring scuffing  results from  over-fueling,
           overheating, or lack of  oil.   Broken piston  rings are  caused by
           the deformation  of the aluminum piston grooves  or overuse of
           Jacobs brakes."(38)

Thus, the expected reduction in engine wear from reducing fuel sulfur content to less
than 0.05 weight percent may not extend  engine life (time  to overhaul), due to the
relative importance of other engine failure  modes.
                                        71

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     4.2    Conclusions From Fleet Data
     From the results of the statistical analyses, it was concluded that there was a
significant decrease in used oil iron content for several engine types between 1984 and
1985-1986.  Anomalies existed in several comparisons of engine types. However, small
sample sizes probably had an effect on the results.  Based on the fleet summaries and
individual engine  comparisons, specifically  the  DDV71  and DDV92  (SCRTD) and
Cummins,  Detroit Diesel  and International Harvester  (Rental Truck  Fleet),   a
consistent  reduction  in used  oil iron content occurred as a  result of lower sulfur
content in the diesel fuel and  other changes such as oil zinc content and new oil TBN.
We cannot extrapolate the reduction  in used oil iron  content to increased engine life.
In addition to the fuel sulfur reduction between  1984 and 1985, other variables which
can affect engine wear were changing.  Oils with different total base number were
used for each year at SCRTD. The lowest average TBN  in 1984 did not go below the
minimum  levels recommended by  engine builders for mandated oil changes (Table 1,
page 22) where wear  rate would be affected by low TBN.  Also, the  oil zinc content
was significantly higher in 1985 and 1986 for oils used by  the  Rental Truck Fleet.  It
appears that the zinc  increase (approximately 28 percent) was not a major contributor
to the decrease in wear metal content, because the lower zinc content oil used in 1984
was still in  a typical  range  for  diesel engine oils and should have provided adequate
wear protection.

     It is, therefore,  concluded that the reduction in diesel fuel sulfur content had  an
effect in  reducing engine wear for some,  but not all of the engine types and fleets
examined.

     4.3    Recom mendations
     Since  neither the literature survey nor the fleet  data completely defined the
effect of low sulfur  fuel on  diesel  engine life,  additional research  is  needed.  The
following recommendations are offered for consideration.

     EPA  should continue to monitor fleet  operation on low  sulfur  diesel fuel.   By
tracking new engines which enter  a fleet operating on low sulfur fuel,  and  eventually
disassembling  and measuring  the wear of representative engines, a determination  of
low fuel sulfur content on engine life can be made.  Oil drain interval extension could
be determined at the same time.
                                       72

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     Another possibility  is to conduct well-defined  engine  dynamometer durability
tests using low sulfur fuel. While very costly, engine dynamometer tests allow control
of variables such as engine load, COT, and oil TEN  so that the fuel sulfur effects can
be isolated and quantitatively determined. Engine manufacturers have procedures for
extrapolating  engine life from durability tests.  Conduct of durability tests using low
sulfur fuel could provide the needed engine life extrapolation.  Engine manufacturers
should be encouraged to use fuel with a maximum  of 0.05 weight percent sulfur for
endurance testing.

      The possible  fuel   lubricity  effect  of  fuel  sulfur  components  should  be
investigated using bench wear tests such as the BOCLE or Cameron-Plint rig.  Results
should determine if the  low sulfur fuel will show a benefit or detriment in this area.
                                        73

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5.    REFERENCES

1.    C.S. Weaver, C. Miller, W. Johnson, and T. Higgins, "Diesel Fuel Quality Effects
      on Emissions, Durability, and Performance:  Preliminary Feasibility and  Cost-
      Effectiveness Analysis for a Nationwide Fuel Quality Regulation," report  under
      EPA Contract #68-01-6543,  Energy and  Resource Consultants, 1985.  Informa-
      tion also presented in  SAE  Paper 860622 "Reducing the  Sulfur and Aromatic
      Content of  Diesel  Fuel:   Costs,  Benefits, and Effectiveness  for  Emissions
      Control," February 1986.

2.    T.A. Tennyson and C.K. Parker, "Locomotive Radioactive Ring Studies of Fuel,
      Lubricant, and Operating Variables," SAE Paper No. 700892, November 1970.

3.    H.R. Ricardo, "Some Notes and  Observations on  Petrol and  Diesel Engines,"
      Diesel Engine User's Association Meeting, 1933.

4.    G.H. CLoud,  and  A.J. Blackwood, "The Influence of Diesel Fuel Properties on
      Engine Deposits and Wear," SAE National F&L Meeting, Cleveland, OH, June 2-
      3, 1943.

5.    C.C. Moore, and W.L. Kent, "The Effect of the Nitrogen and Sulfur Content of
      Fuels on the Rate of Wear in Diesel Engines," SAE Annual Meeting, Detroit, MI,
      January 6-10, 1947, and SAE Transactions, October 1947.

6.    L.A. Blanc, "Effect of Diesel Fuel Characteristics on Engine Deposits and Wear,"
      SAE National F&L Meeting, Tulsa, OK, November 6-7, 1947, and SAE Quarterly
      Transactions, Vol. 2, No. 2, April 1948.

7.    H.M. Gadebusch,  "The  Influence of Fuel Composition on Deposit Formation in
      High Speed Diesel Engines," SAE  National Tractor and Diesel  Engine Meeting,
      Milwaukee, WI, September 1948.

8.    A.G. Cattaneo and E.S.  Starkman, "Fuel and Lubrication Factors in Piston Ring
      and Cylinder  Wear," American  Society  for  Metals Summer  Conference  on
      Mechanical Wear at MIT, June 1948.

9.    R.J. Furstoss, "Field Experience with High Sulfur Diesel Fuels," SAE Quarterly
      Transactions. Vol. 3, No. 4, October 1949.

10.    J.J. Broeze and A. Wilson, "Sulfur in Diesel Fuels-Factors Affecting the Rate of
      Engine Wear and  Fouling," Institution  of  Mechanical  Engineers,  Automobile
      Division, March 1949.

11.    C.F. Perry and W. Anderson, "Recent  Experiences  with  Sulfur in  Distillation
      Type Fuels Burned in U.S. Navy Diesel Engines," Paper No. 74-DGP-4, U.S.  Navy,
      ASME  Diesel and Gas Engine Power Conference and Exhibit, Houston, TX, April
      28 - May 2, 1974.

12.    S.J. Lestz, M.E. LePera, and T.C. Bowen, "Fuel  and Lubricant Effects on Army
      Two-cycle Diesel  Engine Performance," SAE  Paper No. 760717, presented at
      Automobile Engineering Meeting,  Dearborn,  MI, October 1976; also available as
      Interim Report AFLRL No. 80 AD A031885, September 1976.
                                       74

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13.    E.A. Frame, "High Sulfur Fuel Effects in a Two-Cycle High Speed Army Diesel
      Engine," Interim Report AFLRL No. 105, AD A069534, May 1978.

14.    W.C. Gergel, "Trends in Diesel Engine Lubrication Requirements," presented at
      45th Midyear Refining Meeting of American Petroleum Institute, 1980.

15.    3.A. McGeehan, B.3. Fontana, and 3.D. Kramer, "The Effects of Piston Tempera-
      ture and  Fuel Sulfur on Diesel Engine Piston Deposits," SAE Paper No. 821216,
      1982.

16.    3. A. McGeehan, "Effect of Piston Deposits, Fuel Sulfur, and Lubricant Viscosity
      on Diesel Engine Oil Consumption  and Cylinder Bore Polishing," SAE Paper No.
      831721, 1983.

17.    E.A. Frame,  "Fuel Component and Heteroatom Effects on Deposits and Wear,"
      Interim Report BFLRF No.  190, AD A166839, December 1985.

18.    L.V. Malyavinskii and I.A. Chernov, "The Effect of Sulfur  Content in Fuel on the
      Performance  of Engines,"  USSR  All-Union  Scientific  Research Institute of
      Petroleum Industry, Proceedings  of  the  2nd  Scientific  Session  Chemistry of
      Organic Sulfur Compounds in Petroleum and Petroleum Products, 1958 published
      by NSF, 1963.

19.    P.L. Pinotti,  D.E. Hull, and E.3. McLaughlin, "Application  of Radioactive Tracers
      to Improvement of Fuels, Lubricants, and Engines," SAE Quarterly Transactions,
      Vol. 3, No. 4, October 1949.

20.    Letter Mr. G.W. Rossow, Mercedes-Benz  Truck Company, Inc., to Mr. Charles
      Gray, U.S. Environmental Protection  Agency,  December  18,  1986, transmitting
      draft SAE paper on "Diesel Fuel Sulfur and Cylinder Liner Wear of a Heavy-Duty
      Diesel  Engine," E.K. 3. Weiss, B.B.  Busenthuer,  and H.O. Hardenberg.

21.    H.V. Nutt, E.W. Landen, and 3.A. Edgar, "Effect of Surface Temperature on
      Wear of  Diesel-Engine Cylinders and  Piston Rings," SAE Transactions, Vol. 63,
      1955.

22.    D.A. Bolis, 3.H. 3ohnson, and D.A. Daavetilla, "The Effect of Oil and Coolant
      Temperatures on Diesel Engine Wear," SAE Paper 770086,  1977.

23.    3.C. Ellis and 3.A. Edgar,  "Wear Prevention by Alkaline  Lubricating Oils," SAE
      Transactions,  Vol. 61, 1953.

24.    W.C. Gergel,  "Interrelation of Diesel Engine Lubricant Quality and  Sulfur
      Content  of Diesel  Fuel,"  National Petroleum  Refiners  Association Fuels and
      Lubricants Meeting, FL-80-83, November,  1980.

25.    D.  Wei and H.A. Spikes,  "The Lubricity of Diesel Fuels," Wear, Vol. Ill, No. 2,
      September 1,  1986.
                                       75

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26.   Letter,  T.L.  Sprik,  EPA  to  N.R  Sefer,  Southwest  Research   Institute,
      2 October 1986.

27.   "Fight Fuel  Sulfur  -  Your  Diesel's  Silent  Enemy," Caterpillar  Tractor Co.,
      Publication SEBD0598, October 1982.

28.   H.E. Davis, "High Sulfur Fuel-New Diesel Engine Lubrication Recommendations,"
      Caterpillar Tractor Company information letter, June 18, 1980.

29.   Cummins Engine  Company,  "Fuel  for  Cummins  Engines," Bulletin Number
      33769001-03, March 1980.

30.   Daimler-Benz Specifications for Operative Materials, Group 200, Sheet  215.3.

31.   Detroit Diesel Allison, "Fuel and Lubricating Oils for Detroit Diesel  Engines,"
      Bulletin 7SE 270 (Rev. 12-79).

32.   Detroit Diesel Allison, "Fuel  and Lubricating Oils for Detroit Diesel Fuel Pincher
      Engines," Bulletin 7SE 369.

33.   Klockner-Humboldt-Deutz  AG,   Technisches   Rundschreiben,  TR0199-1063E,
      Cologne, 1.9.78.

34.   International  Harvester Company, "High  Sulfur  Fuel  Advisory,"  Bulletin No.
      ESB-79-34, September 1979.

35.   M.A.N., Service Bulletin on Unfavorable Operating Conditions.

36.   Industriale Aditivos do Brazil, S.A.

37.   Translation of Volvo memo to Lubrizol Scandanavia, "Specifications of Longlife
      Oils,"  May 7, 1980.

38.   "Comments  from  API in response to  EPA's  Federal  Register  Requests for
      Comments on Diesel Fuel Quality," (Re 51 FR 23*37, June 27, 1986).

39.   Telephone conversation February  11, 1986,  between E.A. Frame of SwRI and  J.
      Fisher, M. Balnaves, and A. Tuteja of Detroit Diesel Allison.

40.   R.G.  Miller,  Simultaneous Statistical Inference, Mc-Graw-Hill Publishing Co.
      New York, NY, 1966.

41.   J.A. McGeehan, et al., "Some Effects of Zinc Dithiophosphate and Detergents on
      Controlling Engine Wear," SAE Paper No. 852133, 1985.
                                        76

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                                   TECHNICAL REPORT DATA
                            (Please read instructions on the reverse before completing)
1. REPORT NO.
    460-3-87-002
                                                           3. RECIPIENT'S ACCESSION-NO.
4. TITLE AND SUBTITLE
   STUDY OF THE EFFECTS -OF REDUCED DIESEL FUEL
   SULFUR CONTENT ON  ENGINE WEAR
                                                           5. REPORT DATE
                                                             June 1987
                                                           6. PERFORMING ORGANIZATION CODE
7. AUTHOJMS,)
     Edwin A. Frame
     Ruben  A. Alvarez
                               Norman R. Sefer
                                                           8. PERFORMING ORGANIZATION REPORT NO.
                                                           10. PROGRAM ELEMENT NO.
                                                              Work Assignment B-l
9. PERFORMING ORG-\NIZATION NAME AND ADDRESS
    Southwest Research Institute
    6220 Culebra Road
    San Antonio, Texas  78284
                                                           11. CONTRACT/GRANT NO.
                                                               68-03-3353
12. SPONSORING AGENCY NAME AND ADDRESS
    Environmental Protection Agency
    2565 Plymouth Road
    San Antonio,  Texas  78284
                                                           13. TYPE OF REPORT AND PERIOD COVERED
                                                           Final  (9-86/6-87)	
                                                           14. SPONSORING AGENCY CODE
15. SUPPLEMENTARY NOTES
16. ABSTRACT
   The study evaluated wear in heavy-duty  highway-type engines for  reduction of
   sulfur content  of diesel fuel in the  range of 0.50 weight percent  to 0.05 weight
   percent.  A literature review found that  wear rates generally were reduced by
   decreasing  fuel sulfur content.  The  amount of wear reduction was  affected as
   much by operating temperature and engine  load as by sulfur in the  fuel.   Low
   operating temperatures showed more wear at high sulfur levels and, therefore,
   more benefit for low sulfur fuels.  Increasing engine load caused  higher wear
   rates independent of sulfur content.  Lubricant alkalinity (Total  Base Number)
   is effective in controlling corrosive wear at high sulfur levels and reduces
   the potential wear benefit from low sulfur diesel fuel.  Lubricating oil analyses
   from fleets operating on diesel fuel  with less than 0.05 weight  percent sulfur
   were compared with previous data when average sulfur content was 0.35 weight
   percent.  Overall, a significant reduction in engine wear occurred in most engine
   types as measured by iron content of  used oil.  Most of the reduction can be
   attributed  to the low sulfur fuel, with minor contributions from changes in the
   lubricating oils.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lDENTIFIERS/OPEN ENDED TERMS  C. COS AT I Field/Group
   Diesel  Fuel
   Sulfur  Content
   Engine  Wear
   Wear Metals
   Lubricating Oil Analyses
                                               Heavy-Duty Engines
13. DISTRIBUTION STATEMENT
           Release Unlimited
                                              19. SECURITY CLASS (ThisReport)
                                                 Unclassified
21. NO. OF PAGES
    89
                                              20. SECURITY CLASS (This page)
                                                 Unclassified
                                                                         22. PRICE
EPA Form 2220-1 (9-73)

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