EPA-650/4-75-024-b
                        Environmental Monitoring Series
                                  GUIDELIN
     FOR  QUALITY  ASSURANCE PROGRAMS
           FOR  MOBILE  SOURCE  EMISSIONS
                    MEASUREMENT SYSTEMS:
           PHASE I, LIGHT-DUTY  GASOLINE-POWERED VEHICLES -
                                  TEST PROCEDURES
                               U.S. Environmental Protection Agency
                                Office of Research and Development
                                    Washington, 0. C. 20460

-------
                      GUIDELINE DISTRIBUTION RECORD

          EPA-650/4-75-024-b "Guidelines for Quality Assurance-Programs for
          Mobile Source Emissions Measurement Systems:   Phase I,  Light-
          Duty Gasoline-Powered Vehicles" - Test Procedures

     The series of documents, "Guidelines for Quality Assurance Programs  for
Mobile Source Emissions Measurement Systems," have been prepared  and issued in  a
revisable document-controlled format so that any future revisions or additions
may be distributed to the Guideline users.   Individual  copy numbers  have
been assigned to each volume of the series.  These numbers  appear on this record
sheet and on the title page of each document.  The user of  these  documents  must
complete the "Distribution Record Card" and return it in the pre-addressed
envelope to the address shown below so that automatic distribution for future
revisions may be made directly to the user.  Also, notice of any  reassignment
of the documents by number and title to other individuals (by name,  address,
and copy number) should be sent to the same address.

                    U.S. Environmental Protection Agency
                    Office of Mobile Source Air Pollution Control
                    2565 Plymouth Road
                    Ann Arbor, Michigan  48105
                                                                         280
                    ATTN:  Quality Assurance                     COPY No.	


                       (cut along  dotted  line)


                              DISTRIBUTION  RECORD CARD

   Guideline
     User   	  Date	

            Last Name         First          Middle Initial
                              Title

   Address
   to Send  	

   Future                     Street
   Revisions                  btreel
   and      	
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            City              State          Zip Code

   If address is a firm (fill  in) 	
                                             Firm

   I  have received copy No.	of EPA-650/4-75-024-5 "Guidelines for
      Quality Assurance Programs for Mobile Source Emissions Measurement Systems:
      Phase I,  Light-Duty Gasoline-Powered Vehicles" - Test Procedures

   Please send  me any revisions and additions of this volume.

-------
                                     EPA-650/4-75-024-B




                  GUIDELINES


FOR QUALITY  ASSURANCE  PROGRAMS


    FOR MOBILE SOURCE  EMISSIONS


        MEASUREMENT  SYSTEMS:


    PHASE I,  LIGHT-DUTY GASOLINE-POWERED VEHICLES -

                  TEST  PROCEDURES

                         by

          Harold Wimette, Rod Pilkington, and Tom Kelly

                 Olson Laboratories, Inc.              (£ Q (J
                 421 East Cerritos Avenue
                 Anaheim, California 92805


                 Contract No. 68-02-1740
                    ROAP No. 26BGC
                Program Element No. 1HA327


                  EPA Project Officers:

                     R. C. Rhodes
      Quality Assurance and Environmental Monitoring Laboratory
          Research Triangle Park, North Carolina 27711
                         and

                     C.  Don Paulsell
                Office of Program Management
                Ann Arbor,  Michigan 48105


                     Prepared for

          U.S. ENVIRONMENTAL PROTECTION AGENCY
           Office of Mobile Source Air Pollution Control
                         and

              Office of Research and Development
                 Washington, D. C.  20460

                       June 1975

-------
                         EPA REVIEW NOTICE

This volume has been prepared by Olson Laboratories, Incorporated
consistent with the Environmental Protection Agency Quality Assurance
principles and concepts and with the Environmental Protection Agency Mobile
Source Testing Practices at Ann Arbor, Michigan.

The guidelines and procedures are generally applicable to mobile
source testing operations and are intended for use by those engaged in such
measurement programs

It is requested that recipients and users of this document submit any
comments and suggestions to the Project Officers.

Mention of trade names or commercial products does not constitute
Environmental Protection Agency endorsement or recommendation for use.
                    RESEARCH REPORTING SERIES

 Research reports of the Office of Research and Development, U.S . Environ-
 mental Protection Agency, have been grouped into series.  These broad
 categories were established to facilitate further development arid applica-
 tion of environmental technology.  Elimination of traditional grouping was
 consciously planned to foster technology transfer and maximum interface
 in related fields.  These series are:

           1.  ENVIRONMENTAL HEALTH EFFECTS RESEARCH

           2.  ENVIRONMENTAL PROTECTION TECHNOLOGY
           3.  ECOLOGICAL RESEARCH

           4.  ENVIRONMENTAL MONITORING
           5.  SOCIOECONOMIC ENVIRONMENTAL STUDIES

           6.  SCIENTIFIC AND TECHNICAL ASSESSMENT REPORTS
           9.  MISCELLANEOUS

 This report has been assigned to the ENVIRONMENTAL MONITORING
 series. This series describes research conducted to develop new or
 improved methods and instrumentation for the identification and quanti-
 fication of environmental pollutants at the lowest conceivably significant
 concent rations.  It also includes studies to determine the ambient concen-
 trations of pollutants in the environment and/or the variance of pollutants
 as a function of time or meteorological factors.
 This document is available to the public for sale through the National
 Technical Information Service, Springfield, Virginia 22161.

                  Publication No. EPA-650/4-75-02$-b;
                                  11

-------
                           INTRODUCTION
          The test procedures contained in this volume are a docu-
mentation of the 1975 light-duty gasoline emission measurement test
requirements presently in use at the Ann Arbor facility of the Environ-
mental Protection Agency.  These test procedures comply with Federal
Regulations as stated in the Federal Register.  (See Section 3, Vol-
ume I, for the listing of applicable Federal Registers).
          Section 5, Volume I outlines the development of an Operations
manual which may be used as a guideline for a Quality Assurance program.
A typical format of a test procedures manual is described and offers a
guide for implementing and interpreting the test procedures contained in
Volume II.  A user may wish to modify this format to suit specific
contractual obligations or accept the manual in its present form.  The
user will be required to make revisions as needed to assure that the
manual complies with Federal Regulations.  Revisions may be implemented
manually, by computer updates or by magnetic card storage.
          For ease of use, the test procedures are separated into nine
distinct sections, numbered 100-900.  The table of contents shows the
major heading of each section and the test procedures contained in each.
To differentiate between the light-duty and heavy-duty testing which are
both included in this contract, the test procedures are numbered to
correspond to Light Duty, 101-149, 201-249, etc. and Heavy Duty, 150-
199, 250-299, etc.  Light-duty gasoline procedures modified for light-
duty diesel applications are suffixed with a -D, e.g.TP-707-D.
          To assist in defining the overall scope of the light-duty
testing program, the tables from Section 3, Volume I, briefly outlining
the test procedures, specifications and quality provisions are included
in this introduction to the test procedures manual.
          This document details test procedures for light-duty gasoline-
powered vehicles and a subsequent volume will cover test procedures for
heavy-duty diesel engines (Phase II) with a supplement covering heavy-
duty gasoline engines (Phase IV).  The test procedures for light duty
diesel engines  (Phase III) will appear as a supplement to the light-duty
gasoline vehicle procedures detailed in this volume.
                                ill

-------
                     TABLE   OF   CONTENTS
Introduction 	    iii

                                                                      Effective
Section                                                                Date(s)
 100      GAS BLENDING, FUEL ANALYSIS AND INVENTORY.
 101      Preparation of Binary Gas Mixtures .  .  .  .
 102      Calibration of Gas Mixtures	
 200      CALIBRATION	
 201      CVS Calibration	
 202      Dynamometer Calibration	
 203      Gas Analyzer Calibration Curve Generation. .  .  .
 204      Chart Recorder Calibration 	
 205      Temperature Recorder Calibration 	
 206      Barometric Pressure Calibration and Correlation.
 300      VERIFICATION 	
 301      CVS System Verification by Tracer Gas Injection.
 302      Dynamometer Calibration Verification 	
 303      NO  Efficiency Check 	
 304      CO*/H O Interference Check 	
 400      CORRELATION	
 401      Analyzer Cross Check
 500      MAINTENANCE.
 600      DAILY OPERATION	
 601      Log Book Entries . .  .  .
 602      Drift/Noise/Gain/Tune.  .
 603      Test Vehicle Scheduling.
 604      Dynamometer Warm-Up/Set.
 700      EMISSION TESTING 	
 701      Test Vehicle Inspection and Acceptance
 702      Evaporative Emission Preparation .  .  .
 703      LA-4 Vehicle Preparation 	
 704      Test Vehicle Fueling 	
 705      Diurnal Evaporative Test 	
 706      1975 Urban Dynamometer Test - FTP.  .  .
 707      Sample Analysis of 1975 FTP	
 708      Hot Soak Evaporative Test	
 709      Vehicle De-Prep and Removal	
 710      Highway Fuel Economy Preconditioning .
 711      Highway Fuel- Economy Dyno Test - HWFET
 712      Sample Analysis of HWFET 	
 800      DATA VALIDATION.
 801      Data Validation.
 900      PROGRAM PLANNING AND QUALITY AUDIT

-------
                        LIST   OF   TABLES
Table                                                                 Paqe
 1-1      Federal Emission Test Procedure
            Vehicle Preparation and Preconditioning 	  viii
 1-2      Federal Emission Test Procedure
            Evaporative Emission Collection and Measurement 	  x
 1-3      Federal Emission Test Procedure
            Exhaust Emission Test	xii
 1-4      EPA Emission Measurement Facility Organization	xv
                                VII

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                                      Table 1-1.  FEDERAL EMISSION TEST PROCEDURE
                                        Vehicle Preparation and Preconditioning

PROCEDURE
ITEM
BRIEF
DESCRIPTION









FEDERAL
REGISTER
PARAGRAPHS
EPA PROCEDURE
NUMBER
SPECIFICATIONS
AND TOLERANCES
Federal
Register














Engineering
Practice




RECEIVE
VEHICLE
Visual inspec-
tion of test
vehicle to ver-
ify vehicle and
engine system
integrity





85.075-5,6,7


TP-701



None















Refer to manu-
facturers
specific, for
engine class

PRE-
CONDITIONING
AMA
All vehicles
driven over
same route to
establish
similar his-
tories before
test




85.075-7,10,
12
Appendix IV
TP-702



Driving Time-
1 hour. Modified
routes must be
approved by the
Administrator .
Fuel-Tank fuel.
unleaded fuel
0.02 grams of
lead and -0.002
gin. phosphorus
per gallon
minimum.
Leaded Fuel -
1.4 gm. lead
per gallon,
minimum
Urban route ap-
proved by Ad-
ministrator



DRIVE ABILITY

To determine
that veh . is
operating sat-
isfactorily.
safely and can
drive the
federal cycle







TP-702



None















Correct mal-
functions when
possible



VEHICLE
INSPECTION
To assure en-
gine parameters
are correctly
set. Chk IDLE,
CO, RPM, igni-
tion timing
dwell, centri-
fugal and
vacuum advance





TP-701



None















Manufacturers
range or speci-
fication


VEHICLE &
ENGINE
PREPARATION
Leak proof fit-
ting applied to
all fuel sys-
tems. External
vents to permit
collection of
emissions. Fuel
system leak-
checked. Ins tall
thermocouple &
drain tank
85.075-11


TP-702



Fittings and
tubing for can-
isters 5/16
I.D.












Fuel system
should lose
not more than
2" HO at 14"
HO in 5 rain.

TEST FUEL
ADDED
Indolene 30
Indolene HO









85.075-1.0,11


TP-702



See above re-
ferenced para-
graph for de-
tailed specifi-
cations
















PRE-
CONDITIONING
FEDERAL CYCLE
The vehicle is
driven on a dy-
namometer under
controlled con-
ditions






85.075-12


TP-703



Temp 77±9°F
Speed Tolerance
+4 MPH, ±1 sec.
Hot start is
acceptable
















11 HOUR
AMBIENT
SOAK
The vehicle is
stored in a con-
trolled environ-
ment







85.075-13


TP-703



1st hour 81
±5°F. Followed by
10 hours 73
±13°F

















H-
H-

-------
Table 1-1.  FEDERAL EMISSION TEST PROCEDURE
  Vehicle Preparation and Preconditioning
                (Continued)
PROCEDURE
ITEM
QUALITY
PROVISIONS
TEST INVALID
CORRECTIVE
ACTION
TRAINING OR
SKILL
REQUIRED
RESPONSIBLE
OPERATIONS
RECEIVE
VEHICLE
Inspection form
completed and
signed
Engine or vehi-
cle parts
missing or
disconnected
Vehicle re-
turned to
manufacturer .
Engine system
training
Receiving
inspection
Production
Control
PRE-
CONDITIONING
AMA

Failure to
complete route.
Accident.
Reschedule ve-
hicle. Repair
or replace
vehicle.
Normal driving
skills
Testing
Operations
DRIVEABILITY

Engine mal-
function,
brake failure,
vehicle un-
safe.
Return to
manufacturer
or supplier.
Driveability
characteristic
training
Testing
Operations
VEHICLE
INSPECTION
Calibration of
engine test
equipment
Incorrect en-
gine parameters
Adjust under
manufacturers
supervision
Mechanic
Testing
Operations
Support
Operations
VEHICLE fi
ENGINE
PREPARATION

Failure to seal
system. Fuel
system leaks
Return to manu-
facturer
Installation
procedures
training
Testing
Operations
TEST FUEL
ADDED
Color coded
fuel pumps and
vehicle tags
and fuel
inlets. Fuel
analysis
Incorrect fuel
added. Fuel out
of specifica-
tion
Drain tank and
refuel with
correct fuel
None
Testing
Operations
Support
Operations
PRE-
CONDITIONING
FEDERAL CYCLE
Monitor temper-
ature and in-
spection of
drivers trace.
Dyno Calibra-
tion
Temperature
outside limits
Drivers trace
outside limits
Reschedule
test
Dynamometer
cycle drivers
training
Testing
Operations
Support
Operations
11 HOUR
AMBIENT
SOAK
Monitor tempera-
ture in soak
areas
Temperature
outside limits
Starting engine
gine during soak
Reschedule vehi-
cle. Correct
temperature
control .
None
Testing
Operations
Building
Maintenance

-------
  Table 1-2.  FEDERAL EMISSION TEST PROCEDURE
Evaporative Emission Collection and Measurement

PROCEDURE
ITEM
BRIEF
DESCRIPTION










FEDERAL
REGISTER
PARAGRAPHS
EPA TEST
PROCEDURE
SPECIFICATIONS
AND TOLERANCES
Federal
Register













Engineering
Practice






DRAIN
FUEL
Residual fuel
is drained from
tank after 11
hour soak.








85.075-13


TP-702



None













INSTALL CARBON
CANISTER
The carbon can-
ister traps the
emissions from
the fuel sys-
tem. Schematics
A75-3, A75-4,
A75-5, A75-6





85.075-13, 21


TP-702



Capacity-300
±2 ml. Length
to diameter
Ratio-1.4 ±0.1
Inlet and out-
let tubes -
5/16 I.D.,
length 1 inch.
leak tight at
2 PSI 30 sec..
150 ±10 gms.
of charcoal
conditioned
at.30oVf.or

ADD TEST
FUEL
A specified
test fuel with
known composi-
tion is added
to the tank.
Indolene 30 or
Indolene HO





85.002,
85.075-10, 13

TP-702



Charge 50-60°F
Start 60 ±2°F
Q
End 84 ±2 F
Time 60 ±10
min. Charge to
40% of nominal
tank volume to
nearest gallon






DIURNAL
EVAP TEST
HEAT BUILD
Fuel vapors
emitted as a
result of a
specific in-
crease in fuel
tank tempera-
tures in a
specified time
are collected.
Record ambient
and fuel temp-
erature
85-075-13


TP-705



Temperature re-
corder, Range
50-100 ±1°F
Thermocouple -
Type J









(1) For more complete aetail see Federal Register para. 85.075-2;
Fuel pump
cart of not
more than 25
gallon capa-
city. Metts
OSHA require-
ments.







Heating rate
rt
4 ±1.5 F Per
10 min.




Heating blanket
2000 watts to
cover min. 50%
of liquid fuel




DYNAMOMETER
PREPARATION
The vehicle is
placed on the
dynamometer
without start-
ing the engine
and the neces-
sary connec-
tions are made




85.075-13


TP-604



Soak vehicle at
76-86°F for a
min. of 1 hour
before running
loss test










Max. total soak
time from key
off to key on -
20 hours




RUNNING LOSS
TEST
Fuel vapors are
collected dur-
ing operation
of the vehicle
under the spec-
ified test
schedule





85.075-13


TP-706



See 1975 ex-
haust emission
test Table 1.3
Vapors are not
collected dur-
ing 10 Bin soak
or 505 second
"hot" start
test






See Table 1.3







1 HOUR HOT
SOAK LOSS
Fuel vapors are
collected for 1
hour beginning
immediately
after the en-
gine is turned
off.





85.075-13


TP-708



Ambient top.
76-86°F





















auasTER
HEIGHT
The collected
vapors are de-
termined by
weighing the
canister before
and after the
test.





85.O75-27


Tl»-70e



Weighing accur-
acy equip ±75 ng
weight deter-
mined to 20 mg.











Metier F1200 or
equivalent Reada-
bility 0.01 gram





-------
  Table 1-2.  FEDERAL EMISSION TEST PROCEDURE
Evaporative Emission Collection and Measurement
                  (Continued)

PROCEDURE
ITEM
QUALITY
PROVISIONS







TEST
INVALID





CORRECTIVE
ACTION




TRAINING OR
SKILL REQUIRED





DRAIN
FUEL
Check-off sheet
signed by
witness






Failure to
drain tank.
Starting
engine .



Reschedule





Basic know-
ledge of fuel
system.




INSTALL CARBON
CANISTER
Installation
checked by team
leader . Canister
checked for
leaks by
comparing wt.
before test
with previous
tare weight.
Improper in-
stallation or
canister leaks




Correct in-
stallation. Re-
schedule if
heat build
had been
started.
Familiarity
with EPA ap-
proved in-
stallation
for engine
family
DIURNAL
ADD TEST EVAP TEST
FUEL HEAT BUILD
Ambient and fuel temp. Record
checked by data validation (DV)
step by step procedure check-
off form signed by witness





Incorrect temperature, heating
rate or time of heat applica-
tion.




Reschedule





Basic knowledge of heating and
temp measuring equipment.





DYNAMOMETER
PREPARATION
Ambient temp.
and soak time
by DV.






Failure to
preset dyno-
mometer load or
warm up dynano-
mometer Incor-
rect ambient
temperature
Reschedule





Knowledge of
dyno procedures





RUNNING LOSS
TEST
See
Table 1.3







Failure to
follow driving
cycle within
prescribed
tolerances . See
also Table 1.3

Reschedule





Trained driver
See Table 1.3





1 HOUR HOT
SOAK LOSS
Ambient temp.
record checked
by DV






Failure to
reconnect can-
isters after
"hot" start
test . Incorrect
soak temp.

Reschedule
evap. only.




Knowledge of
canister in-
stallation




CANISTER
WEIGHT
Data checked by
D.V.







Negative weight
gain is suspect .





Reschedule
using freshly
dried or new
canister


Knowledge of
balance
operation.




-------
Table 1-3.  FEDERAL EMISSION TEST PROCEDURE
           Exhaust Emission Test
PROCEDURE
ITEM
BRIEF
DESCRIPTION










FEDERAL
REGISTER
PARAGRAPH
EPA
PROCEDURE
NUMBER
SPECIFICATIONS
AND TOLERANCES
Federal
Register


























DYNO WARM-UP
AND HP SETTING
The vehicle is
placed on the
dynamometer
which has been
previously
warmed up and
the hp set





Appendix II
85.075-15


TP-604



Less than 2 hrs
between tests -
warm-up - 15
min @ 30 MPH
within 1 hour
of test. Hp
setting - any
time prior to
test. For auto
1 hour prior
for manual. In-
flate tires to
45PSI. Use
vehicle re-
straint to
minimize rock-
ing.











CONSTANT VOLUME SAMPLER (CVS)

CALIBRATION:

The positive
displacement
pump is cali-
brated using a
laminar flow
element or
equivalent.



Appendix III



TP-201



See Appendix
III for equip-
ment toler-
ances . Measure
actual pump
cavity pres-
sure/tempera-
ture variation
during calibra-
tion ±2 F grad-
ual change .
Leak- free con-
nections.















OPERATION:

An integrated
portion of the
total exhaust-
air mix is
collected
during the
driving cycle
along with a
sample of dil-
ution air.
85. 075-20, -24



TP-706



CVS inlet
pressure less
than 1 in H2O
Heat exchanger
±10 degrees of
set point temp
ace. ±2°F.
Flow rate 300-
350 cfm. Dilu-
tion filters
consisting of
a charcoal
filter between
two particu-
late filters
Press, guage
±3 mm. Bag
sample flow
rate 10 cfh.
min. Specific
sampling pro-
cedure FR-24.






DRIVING
CYCLE
A driving cycle
typical of ur-
ban driving is
performed on
the dyno
according to
the FR driving
schedule.




Appendix I
85. 075-14, -15,
-19, -24

TP-706



Horsepower
setting - see
FR-15. Fan 18-
12 inches in
front or to
provide suffi-
cient cooling.
Driving trace
precision - ±2
mph within 1
sec. Shift
points - see
FR-16-17. En-
gine shutdown
at 1369 sec-
conds . Time
between cold
and hot tests
10 ±1 minute
Engine starting
FR-19 Ambient
o
Temp 68-86 F






ANALYTICAL SYSTEM

CALIBRATION :

Primary gas
standards are
used to estab-
lish the in-
strument curve





85.075-23



TP-203



Calibration
performed every
30 days. Zero
gas impurity :
1 ppm HC
1 ppm CO
400 ppm CO
0 . 1 ppm NO
0 13-21 mole%
(AIR)
Calibration
Points :
HC S NO 50 &
100%
CO & CO -
10, 23, 40, 50,
60, 70, 80,
100% of full
scale. Analysis
of gas ±2% of
actual value.
Curve construc-
tion - best
judgement.
Analyzer warmup
- HC - 20 min.
CO, C02, NO -
2 hours
OPERATION:

The bag sam-
ples collected
by the CVS are
analyzed for
CO, CO , HC and
NO .
X



85. 075-23, -24



TP-707,711



Analysis per-
formed within
20 minutes from
end of sampling
Zero and span
instruments be-
fore and after
sample measure-
ment. Span gas
should have cone
of 80% of full
scale.
















DATA
COLLECTION
Ambient condi-
tions are re-
corded along
with instrument
outputs and
operating par-
ameters . Vehicle
and test cell
identification
and other per-
tinent informa-
tion.
85.075-22,25



TP-707



All information
is recorded ac-
cording to mea-
surement speci-
fications .























DATA
REDUCTION
The grams per
mile are calcu-
lated for each
component using
the formula in
the FR






85.07-26



TP-801



Reported to
three signi-
ficant figures
Density at 68°
1 atm.
HC 16.33
NO 54 . 16
COX32.97
CO 51.85




















-------
Table 1-3.  FEDERAL EMISSION TEST PROCEDURE
           Exhaust Emission Test
                 (Continued)
PROCEDURE
ITEM
SPECIFICATIONS
AND TOLERANCES
(Continued)
Engineering
Practice













QUALITY
CONTROL
PROVISIONS













DYNO WARM-UP
AND HP SETTING



Allowable
horsepower var-
iation less
than ±0.5 hp.











Calibration
performed
monthly with
weekly checks.
Correct setting
for vehicle
weight checked
by data valida-
tion (DV) . Time
of previous
test run is
checked for
dyno warm-up
requirement.


CONSTANT VOLUME SAMPLER (CVS)



CALIBRATION:















Propane injec-
tion must agree
within ±2% of
calculated
value. Daily
propane injec-
tions plotted
on control
charts. Inter-
nal check of
calibration
data for uni-
formity.





OPERATION:
Tailpipe ±5 in
H_O. Sample mix
temp, at pump
inlet 90-115 F
Heat exchanger
±5°F of set
point.
Dilution inlet
air 65 F rain.
P. 70" H20 max.
Bag construc-
tion 5 f ted-
lar film.


Weekly perfor-
mance checks
of equipment
Specifications
DV checks each
test for out-
of-control
operating
conditions .







DRIVING
CYCLE



Preprinted or
computer traced
driving sched-
ule. A minimum
of 12 hour and
maximum of 20
hour soak from
key off to key
on.






DV checks
speed, time.
trace, crank.
time, amb. temp
and all record-
ed information.
Daily span
check of driv-
ing aid. Driver
performance
audit.





ANALYTICAL SYSTEM




Calibration
points: CO, CO,
5 points & 0
across each
range. Curve
construction -
within ±2% of
each point
value, smooth
curve passing
through zero
(origin) .
Weekly
calibration
check.
Calibration gas
analysis trace-
able to EPA
gravimetric
blends and/or
NBS-SRM's.
Inter-labora-
tory gas cross
check. Annual
restandardiza-
tion of gases.
Monthly instru-
ment perfor-
mance checks.
CVS gravimetric
injections.



Digital volt-
meter readings
of instrument
output record-
ed on chart.
Zero repeated
after each span
adjustment







Bags are leak
checked before
each test. NO
converter effi-
ciency check
performed daily
Analytical
system given
monthly per-
formance in-
spection and
preventative
maintenance
recorder
checked against
DVM each test.
DATA
COLLECTION


















DV inspects all
recorded infor-
mation for
spurious re-
sults and
facilitates
the smooth and
timely flow of
test documenta-
tion.






DATA
REDUCTION



NO and N02 re-
ported separate-
ly corrected and
uncorrected .











Data reduction
is usually per-
formed by com-
puter. Manual or
independent
check of the re-
duction program
should be per-
formed monthly &
whenever change
in program. Com-
puter output
checked by DV
for corrections.



-------
Table 1-3.  FEDERAL EMISSION TEST PROCEDURE
           Exhaust Emission Test
                (Continued)
PROCEDURE
ITEM
TEST
INVALID









CORRECTIVE
ACTION






TRAINING
OR SKILL
REQUIRED





DYNO WARM-UP
AND HP SETTING
Failure to
wannup dyno.
Incorrect hp
setting for
weight. Vehicle
exhaust not
connected to
CVS.



Reschedule







Dyno operation







CONSTANT VOLUME SAMPLER (CVS)

Calibration in-
valid if pro-
pane injection
out of spec.







Repeat propane
injection. Re-
fer to Appendix
III for trouble
shooting.
Repeat calibra-
tion.

Special train-
ing in use of
calibration
equipment .
Experience in
emission
testing.

CVS flow rate
too low - in-
correct pump
speed used.
Equipment
failure or out
of spec.
Filters
plugged.


Reschedule







Special train-
ing in CVS op-
eration. Fami-
liar with
other test
equipment and
procedures .

DRIVING
CYCLE
Driver outside
specified lim-
its during
cycle . Improper
starting -
stalling proce-
dure. Out of
spec time
sequence. Soak
period to long
or short .
Reschedule
Driver perfor-
mance audit may
be necessary




Trained in
special driving
skills required





ANALYTICAL SYSTEM

Incorrect Stan-
dards or data
used to con-
struct curves.







Repeat calibra-
tion. Generate
new curve when
data points out
by more than
±0.5% deflec-
tion.

Special train-
ing in calibra-
tion procedure.
Previous exper-
ience as system
operator
desirable.

Leak .in sample
bag detected
may invalidate
previous test.
Incorrect span
setting instru-
ment malfunc-
tion such as
span drift.


Repair or re-
place sample
bag . Reschedule
previous test .
Reschedule if
equipment fail-
occurs .

Training, in
analytical sys-
tem operation.
Knowledge of
test procedures



DATA
COLLECTION
Incorrect data
or information









Correct infor-
mation when
possible. Re-
port all data
and information
errors. Resche-
dule if data is
not correctable
Data validation
should be
familiar with
test procedure.
basic statisti-
cal and techni-
cal knowledge
is desirable.
DATA
REDUCTION
Computer program
or data input
incorrect.








Correct program
or data input
and repeat cal-
culation .




Computer pro-
graming capa-
bility required
if done in-
house . Computer
operations
training .


-------
                EPA  EMISSION  MEASUREMENT  FACILITY ORGANIZATION
                         OFFICE  OF PROGRAM MANAGEMENT
                                  DIVISION
                                  DIRECTOR
                   QUALITY
                 ASSURANCE
         ADMINISTRAT
              BRANCH
 VE
                            PROGRAM
                            ANALYSIS
LABORATORY
  BRANCH
PRODUCTION
 CONTROL
SCHEDUL
NG
COORDINATION
    DATA
 VALIDATION
                                     DATA
                                    BRANCH
  TESTING
 OPERATIONS
                        LIGHT
                        DUTY
    HEAVY
    DUTY
EVALUATION &
DEVELOPMENT
           FACILITIES
             SUPPORT
                         EOUIPMENT
                        MANAGEMENT
            CHEMISTRY
PLANNING
SECTION
                                 EQUIPMENT
                                   DESIGN
DRAFT
ING
          CORRELATION
         5- MAINTENANCE
                                            INSTRUMENT
                                            SERVICES
                                               RTS
                                            ELECTRONICS
                                               CRAFT
                                             SERVICES
                                  Table 1-4
                                     xv

-------
100

-------
               Section 100
GAS BLENDING, FUEL ANALYSIS AND INVENTORY

-------
EPA TEST
SUBJECT
PREPARATION OF
Reference
c.
Number
PROCEDURE Tp_101 page , of ln i
GRAVIMETRIC BINARY GAS MIXTURES
Data Form No.
D. PAULSELL DRAFT 8/1/73 101-01, 02
Responsible Organization Computer Program i
CHEMICAL ANALYSIS CYLBLEND '
Test Witness Performance Interval
QUALITY ASSURANCE REVIEW/REQUESTOR AS REQUESTED
Type of Test Report Supersedes ;
GAS BLEND DATA SHEET NEW i
Report Distribution Superseded by i
QUAL. ASSUR. , CORR. & MAINT. , INST. SERV. >
REMARKS/ COMMENTS

Office
PROGRAM MGNT
LAB. BRANCH
LAB . BRANCH



Change
Letter
ORIGINAL RELEASE APPROVALS
Section Signature
QUALITY ASSURANCE
CHIEF
SUPP . OPERATIONS CHIE ?


Date





REVISIONS
Description of Change Approval

Date


-------
REVISIONS:


PREPARATION OF GRAVIMETRIC BINARY
GAS MIXTURES
TEST PROCEDURE
PROCEDURE NO.
TP-101
pAftF 2 OF 10

1.0  PURPOSE

     This procedure outlines the equipment, blending process, and calculations
     necessary to generate binary gravimetric gas mixtures to be used as pri-
     mary standards.  The gravimetric technique is considered to be the most accu-
     rate method for the quantification of gases.  Since the final data re-
     ported for emission measurement is in mass units it is of great impor-
     tance that the primary standards be determined by mass rather than
     pressure or volumetric relationships.

2.0  TEST ARTICLE DESCRIPTION

     Binary mixtures are prepared from pure components or blending mixtures of
     propane  (C3Hg), carbon monoxide  (CO), carbon dioxide (C02) and nitric
     oxide  (NO).  Dilution of these gases is done with pure nitrogen or air.

3.0  REFERENCES
     3.1  Procedure For Making Gravimetric Binary Gas Mixtures.  EPA,
          C.D. Paulsell, 8/1/73.

     3.2  Matheson Gas Data Book

     3.3  "The Present State of The Art In The Preparation of Gaseous Standards",
          Scientific Gas Products, Inc.

     3.4  "Handbook of Compressed Gases", Compressed Gas Assoc., Inc. Rein-
          hold Publishing Corp., New York, N.Y.
4.0  REQUIRED EQUIPMENT

     4.1  Cylinders:
     4. 2  Valves:
     4.3  Balance:
     4.4  Weights:
Marison  1CC3AA1800 Carbon Steel
5.25" O.D. x 13.75" Length Volume -
223 Cubic Inches
                         Stainless Steel NOX Cylinders
                         3.75"  O.D.  x  13.0" Length
                         Volume - 110 Cubic inches
Brass, Sherwood Selpac B
G-5 3540 F9  CGA350

Stainless Steel Superior
CGA 660SS

Voland Model 1115 CDN
lOKg Capacity
1 Mg Accuracy

2 sets (1 gram to 1 kilogram)
Calibration traceable to NBS

-------
REVISIONS:

PREPARATION OF GRAVIMETRIC BINARY
GAS MIXTURES
TEST PROCEDURE
PROCEDURE NO.
TP-101
PAGF3 OF 10 ..
     4.5   Blending  manifold with  pressure  gauges  to  cover 0-30,
          0-300,  and 0-2000 PSIA  and (1) vacuum gauge  0-5 PSIA

     4.6   Vacuum Pump:    150  liter/min maximum capacity
                         Ultimate pressure 1 millitorr Hg absolute.

     4.7   Pure Gases

          o    Zero grade Air:      220-300 cubic  feet
                                   2000-2600 P.S.I.G.
                                   Max.  THC 0.1  PPMC
                                   02 19-23% Analyzed

          o    Zero grade Nitrogen:      220-300 cubic  feet
                                        2200-2600 P.S.I.G.
                                        Max. THC   0.1  PPMC

          o    0_ free nitrogen for NO blend

          o    Propane - Instrument Grade  99.5% minimum

          o    Carbon Dioxide - Coleman  -  99.8% minimum

          o    Carbon Monoxide -  Ultra high purity - 99v8%
                                 THC  1  PPMC

          o    Nitric Oxide,  C.P. Grade,  99.0% Min.

5.0  PRECAUTIONS

     5.1   Gas blending should be  attempted only by qualified personnel famil-
          iar with the chemistry  of gases  and  blending equipment operations.
          Equipment damage, serious injury, or loss  of life could occur from
          deviations from prescribed practices.

     5.2   Personnel should be familiar with safe  handling of compressed gases

     5.3   Avoid sudden surges of  gases when blending or  transferring.   Always
          "Bleed" gas slowly from one cylinder to another in order to minimize
          temperature changes.

     5.4   Special precautions should be  taken  when blending combustible gases
          such as propane and CO  with air. Only  very  low concentrations
          should be attempted i.e.,  less than  1000 PPM.

     5.5   Attach only the diluent being  used to the  blending manifold (air
          or nitrogen).

     5.6   All traces of combustible material such as oil, grease, and solvents
          shall be removed from the gauges, fittings,  valves and tubing contained
          in the blending manifold.   All manifold parts  should be specified,
          "cleaned for oxygen service,"  when ordered.

-------
REVISIONS:


PREPARATION OF GRAVIMETRIC BINARY
GAS MIXTURES
TEST PROCEDURE
PROCEDURE NO.
TP-101
PAOF 4 OF 10

     5.7  Cylinder valves should be inserted with teflon lubricant only.

     5.8  Never drop cylinder or weights onto balance pans or release quickly.

6.0  VISUAL INSPECTION

     6.1  Cylinders:

          o    Check for valve or cylinder damage, especially the threads on
               the valve.

          o    Check the cylinder for dirt or other contamination

     6.2  Blending Manifold:

          o    Check all tubing and the cylinder connections for loose or
               damaged fittings.

          o    Check gauges for proper atmospheric reading.

     6.3  Balance:

          o    Check for any visual damage.

          o    Check weights for damage or contamination.

7.0  PREPARATION

     7.1  Weights:

          Remove all weights from the balance pans and case, dust them care-
          fully and wipe any smears from the weights with a lint free cloth.
          Do not touch with hands.

          The weights should be kept in their box when not in use and should
          only be handled with the transfer tool provided.

     7.2  Balance:

          Turn the vernier chain mechanism to zero and release the pans of
          the balance.  Check the action of the pan arrest pads and adjust
          if necessary to achieve smooth operation.  When the pans are stable,
          the indicator should read null.  If it does not, adjust the zero
          knob to bring the needle to the null position.  Arrest and release
          the pans several times to assure that the balance stabilizes in the
          null position.  The balance point for the loaded pans should be
          within ±10 mg.
                                        7

-------
REVISIONS:

PREPARATION OF GRAVIMETRIC BINARY
GAS MIXTURES
TEST PROCEDURE
PROCEDURE NO.
TP-101
PAr,F 5 np 10
     The weights are now ready to be  cross  checked  on the  balance  to
     assure accurate determination under  loaded  conditions.   Place the
     weights in the center of the pans  as indicated below  and note any
     deviations.
                       £eft Pan
                          0
                          1
                         1,  2
                         2,  3
                        2, 3,  5
                     2,  3, 5,  10
                       10, 20
                      20,  30,  2
                     20,  30, 50
                          0
                   20,  30, 50, 100
                      100, 200
                      200, 300
                    200,  300,  500
                          0
   Right Pan
        0
     Vernier
        3
        5
       10
       20
       30
50,  1, Vernier
      100
        0
      200
      300
      500
     1000
        0
7.3  Cylinders:
     New cylinders or cylinders which have been recently revalved should
     be checked for leaks  by pressurizing to 1800 PSIG with nitrogen.
     Some leaks are not apparent until the cylinder has reached its maxi-
     mum pressur  distortion.  Check for leaks with "Snoop" or other de-
     vice which will not leave a residue on the cylinder.  Check valve
     stem, relief device and cylinder threads.  Note results in cylinder
     log.  Correct leaks if possible.  If valve is leaking at the cy-
     linder threads, the valve must be removed and reinserted.  Do not
     attempt to tighten valve.

     Cylinders  which have  previously been used for mixtures should be
     flushed with the diluent  (air or nitrogen) as follows:

     o    Vent  cylinder contents slowly in the hood being certain the
          hood  blower is operating.

     o    Evacuate to 1.0  PSIA.

     o    Fill  to 15 PSIG  (30 PSIA) with diluent to be used.

     o    Vent  the contents and evacuate.  Repeat this purge to final
          evacuation 0.2 PSIA.

     o    Confirm that cylinder pressure is less than 0.2 PSIA.

     o    Close cylinder valve firmly and proceed to the blending
          procedure.

                                8

-------
REVISIONS:
PREPARATION OF GRAVIMETRIC BINARY
GAS MIXTURES

  TEST    PROCEDURE
PROCEDURE NO.
     TP-101
                                                               PAGEJL-OF
           10
      7.4  Blending Manifold:

           With all vents closed on the  manifold, pressurize all gauges to
           25 PSIA and close off the manifold.  Check all gauges for corre-
           lation and observe the readings for indicating leakage.  Find and
           correct any leakage.  This is especially important in preparation
           of NO blends.  Small oxygen leaks will oxidize the NO to NO2 and
           this can occur at manifold pressures above atmospheric.  Leakage
           of the NO gas should be avoided because of its toxicity and
           transfer should be performed  in a hood or well ventilated area.
                                      9

-------
REVISIONS:


PREPARATION OF GRAVIMETRIC BINARY
GAS MIXTURES
TP^T PROCEDURE
1 CO 1 I l\VXV»t i< Wl\k
PROCEDURE NO.
TP-101
pAftF 7 np 10

8.0  TEST PROCEDURE

     The preparation of gravimetric gas mixtures basically involves two
     procedures, blending and weighing.  Blends are made according to the
     information contained on Form No. 101-01.  This form must accompany
     the work order and be completed by the requestor.  Refer to Reference
     3.1 for calculation procedures.  Test data is entered on Form No.
     101-02.
Test Sequence
     101
     102
     103
     104
     105
     106
              Test Description

   Parent Blend Made From Pure Component

Evacuate and purge with diluent (N2 or Air,
whichever will be used in the mixture) twice and
then evacuate the cylinder to 0.2 PSIA.  Close
the cylinder valve and remove the vacuum line.

Wipe cylinder to remove the dust and place on
the left pan of the balance.
Place a similar type cylinder on the right pan
to compensate for buoyancy.  This same cylinder
must be used for all subsequent weight deter-
minations.  Record cylinder number in blending
log book.

Add weights to right pan until null indicator
shows a deflection.  This will indicate that the
null is within 1 gram of the weight.  NOTE:  If
the blending cylinder should weigh less than the
tare cylinder a weight must be added to the left
pan.  Do not remove this weight until all weigh-
ings have been completed.

Close balance door and obtain final null with
vernier chain.  Record sum of wts. on right bal-
ance and null vernier indicator weight.  Secure
and release pans to assure zero null.

Attach the cylinder to the minor component regu-
lators.  (This line should be equipped with a
flow control valve.)  Purge the line with the
minor component up to the empty cylinder valve.
Data Output
   None
   Record
   cylinder
   number
                                                                         Log Book
                                                                         Entry
                                                                         None
                                                                         Cylinder
                                                                         Weight
                                                                         Grams
                                       10

-------
REVISIONS:
        PREPARATION OF GRAVIMETRIC BINARY
        GAS MIXTURE

            TEST    PROCEDURE
PROCEDURE  NO.
    TP-101	
PAGE JL.OF  10
 Test Sequence
      107
      108
      109
      110
      111
      112
              Test Description

Set the regulator on the minor component to
the pressure indicated under column shown
P! PSIG on form 101-01.   If pressure is less
than atmospheric the blending manifold must
be used and cylinder is filled using the
pressure indicated under PSIA.

With the flow control valve closed, open the
cylinder valve.  Bleed in the desired amount
of pure component.  If above atmospheric allow
the cylinder to attain equilibrium with the
regulated pressure.

Close the cylinder valve, and shut off minor
component.  NOTE:  To achieve 0.1% accuracy
always add at least 5 grams of minor
components.  Reweigh the cylinder as in
Sequence 102-105.

The cylinder is now ready for the addition of
diluent.  The cylinder is attached to the gauge
manifold and the lines are purged with diluent
up to the CGA fitting.  When the 0-2000 PSIA
gauge reaches a pressure higher than that of the
cylinder  (200 PSI),  open the cylinder valve and
fill it by regulating the diluent in 100 PSIA
increment.  Close the cylinder valve when the
pressure gauge needle moves past the desired final
pressure.  The final pressure should be approxi-
mately 3% final pressure higher than desired to
makeup for the pressure loss due to the cylinder
cooling.

Shut off the diluent source and bleed the mani-
fold before disconnecting the cylinder.  Reweigh
the cylinder as in sequence 102-105 after the
cylinder has reached ambient temperature.

Record the three weights and submit the data for
computation of mass ratio, concentration, and
final pressure.
    Data Output
      Weight
      after
      adding
      minor
      component

      None
      Weight
      after add-
      ing Major
      Comp.Grams

      Initial
      Minor
      Final
                                      11

-------
REVISIONS:
      PREPARATION OF GRAVIMETRIC BINARY
      GAS MIXTURES

           TEST     PROCEDURE
PROCEDURE NO.
  TP-101	

PAGE_10F 10—
 Test Sequence
      113
      114
             Test Description

The parent blend should be mixed thermally for
1/2 hour by directing a heat lamp from a
distance of 18-24 inches at the bottom of the
cylinder which has been tilted 45 with the
horizontal.

If a dilution of the parent mixture is to be
made, the same procedure is used except that the
parent blend can be added to the empty cylinder
by using a well purged regulator to obtain the
approximate pressure needed to achieve the final
concentration desired.
    Data Output
                                     12

-------
REVISIONS:


PREPARATION OF GRAVIMETRIC BINARY
GAS MIXTURES
TEST PROCEDURE
PROCEDURE NO.
TP-101
PAGE_ULOF m
9.0  DATA INPUT

     Form 101-02 requires the following:

          Blending  Date
          Components
          Operators Initials
          Cylinder Numbers
          Cylinder weights  (3) Initial, Minor, Final
          Comments

10.0 DATA ANALYSIS

     10.1 Submit data for analysis by "CYLBLEND" computer program.

11.0 DATA OUTPUT

     11.1 Computer print out showing calculated mass ratio concentration.
          Forward with complete job request to requestor.

     11.2 Compare specified value with calculated value.  Check final cylinder
          pressure.

     11.3 Check computer entries against original data form.

     11.4 If cylinder was previously used, check to see that it has been
          deleted from the inventory list.

12.0 ACCEPTANCE CRITERIA

     12.1 Calculated values should agree with specified within +_5%.  If not
          determine cause and if final concentration is acceptable, correct
          and report the errors or failures.

13.0 QUALITY PROVISIONS

     13.1 See Section 7.2 balance check.

     13.2 NBS certified weights are used to check the working weights at
          six month intervals.

     13.3 Gases used for blending are checked for purity when received from
          supplier.
                                       13

-------
                    GRf\\MMETR\C  eA
                                           P/VrA
Ncf.V.N AU
CCrO-CENTR/VTl^


:







COM?.
NMN&R
MA-31K









fM^oft.
oLE^D
R^Q'D.









C>?CN.^
I ?\ U O ~J .
P '
' !
"- -^ \ rt- _
s •--• i vj









PRUSS.
O
• }
PS I A







!
1
AFPRC.X.
^ ^
IM|
GKhC-'lS



















i
PRESS.
p.
PS! A









APPRcX.
M -.
GRr^AS









MAf^iSoNi
CVL.SpRiAL MO.
USE D




.. -




\oi-oi

-------
                                         GRAVIMETRIC GAS BLENDS
                                           INPUT DATA SHEET
BLENDING
DATE


•»


-




COM
MINOR




PC
JMENTS
MAJOR






BLENDERS
INITIALS




                                                     CO
                                             MINORS
                                                                          COMPONENT SYMBOLS
                                                    NO
                                                    CH4
                                                                           PROPANE        (99.5%. MIN.)
                                                                           CARBON MONOXIDE
                                                                           CARBON DIOXIDE
                                                                           NITRIC OXIDE
                                                                           METHANE
                    50l
                                                             MAJORS
                                                    AIR  - ZERO GRADE AIR
                                                    N2   - ULTRA PURE NITROGEN
Q
_J
C3





-

I
2
3
i|
r
j
6
7
2
CYLINDE
NEVI
BLEND
f


-
-









-
-
-
-
-


-





-





















-
-

S| ,0
R NUMBERS
PARENT
BLEND
n
-

-


-

-
-
^^
-








-
-

-

-













-





INITIAL i
(EMPTY)
Zl




-










>S| 20






-
































35






-
AFTER
ADDING
MINOR





































	


1—













AFTER
ADDING
MAJOR
37
-





30| 3S







































40








-











-

_ COMMENTS:
















4$
















































































50| 5S








































60
































































































































































65) 70! 75 | SO
M NOTES: TWO SPECIAL PARENT CYLINDER NUMBERS ARE RECOGNIZED.
^ " -PURE " INDICATES A PARENT BLEND HAS BEL'is MADE FROM PURE COMPONENTS.
" -VKUT " IMr>IC7vTES THAT THE CYLINDER REFERENCED HAS BEEH VENTED AND
MTS COMMAND:
       IS TO BE  DELETED FROM THE FILE  OF CYLINDERS.

$ RUN  SAQF: CYLBLEND.  [SCARDS = *SOURCE*]  [SPRINT = *SINK*]
DATA SETS >TUST  BE SEPARATED BY A SINGLE $  ENDFILE CARD.
TOTAL  RUN TERMINATES ON TWO $ ENDFILE CARDS.
   Form 101-02

-------
                                                            TP-101
                                                            Attachment No.
                            EPA STANDARDS  INVENTORY
Propane in Air
    3
    5
   10
   15
   25
   50
   75
  100
  150
  200
  275
  350
  500
 1000
ppm *
ppm
ppm *
ppm
ppm
ppm *
ppm
ppm *
ppm
ppm
ppm
ppm
ppm *
ppm
Methane in Air

    3 ppm
   10 ppm
   25 ppm
   50 ppm
   75 ppm
  100 ppm
  300 ppm
 1000 ppm
20000 ppm P/N2
GRAVIMETRIC GAS
CO in N0
5 ppm
10 ppm
25 ppm
50 ppm*
100 ppm*
150 ppm
200 ppm
250 ppm
500 ppm*
750 ppm
1000 ppm*
1250 ppm
1500 ppm
2000 ppm
2500 ppm
3000 ppm
4000 ppm
0.5%
1.0%
1.5% P
2.5%
5.0%
7.5%
10.0%
BLENDS
CO0 in N?
0.2%
0.4%
0.6%
0.8%
1.0%*
1.5%
2.0%
2.5%
3.0%
4.0%
5.0%
7.0%
9.0%
11.0%
13.0%
15.0%*








NO in
25
50
75
100
250
500
750
1000
1500
2000
5000
20000
N?
ppm
ppm *
ppm
ppm *
ppm *
ppm *
ppm
ppm *
ppm
ppm
ppm
ppm
Propane in N-,
  100
  200
  400
  600
  800
 1000
 2000
 3000
 4000
 6000
 8000
 10000
 15000
 20000
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm
ppm P
ppm
ppm
  NOTE:   The concentrations shown here
         are the nominal values (+0,-10%)
         which are to be generated,
         inventoried, and maintained as
         gravimetric standards.

SYMBOLS:  P = Parent Blend
          * = NBS Standard
                                      16
                                                           Revision Date

-------
            GRAVIMETRIC (sAS  HLLNO  ANALYSIS
                                                               TP-101
                                                               Attachment No. 2
                    DATE:  qs- 11 -74
                          'jrt,
MEASURED DATA:

                  PARENT
CYLINDER NO.  CYLINDER NO.
                          MINOR  COMPONKNT:  co
                          MA JO*  COMRONFNT:  Na«»{>
(GRAr^S N2 )


344.556
MASS
RATIO
•»«••!)• •>>•»•»•«••&•» '
1


0.0191777
BLEND
CONC.
•B- C- v- •»• C- -O -U- -vi- •«•
(RHM)


19181.750
CYL.
PRESS.
«• •» -u * «• « « •»
(RblA)


1230.
COMMENTS DATA


CYLINDER NO.
  {!••»««•&•«•«•<

  6-11865
  G-11832
  G-11632
USED F0« CH4 / C3HM RLEND
 ***CYLIMOEK NOT FOUND.
ERROR IN PREVIOUS BASSES
99.5V: PU«E SCOTT ^-354
           PROCESSED:   08:45.o'o   VAY  14,  1974
                      17

-------
                    «»« GHAVlMt. TKIC
                                        tiLt'Nl) ANALYSIS
                             TP-101
                             Attachment No. 3
                   DATE*. OS-11-74     MINOR COMPONENT:  CO
                BLENDER:  JK          MAJOR COMPONENT:  N2
MEASURED DATA:
CYLINDER NO
                 PARENT
                       NO.
   MEASURED CYLINDER WEIGHTS:
EMPTY     AFTER MINOR  AFTER MAJOR.
  F-01363
  F-01364
  F-01366
  F-01367
  F-01369
  F-01370
  F-01372
  F-01374
CALCULATED DATA:
                  -PURE
                 G-11864 .
                 G-11832
                  -PU^E
                  -PURE
(GRAMS)
111.534
145.703
127.413
117,
 10,
 74,
 63,
   401
   725
   364
   287
                  -PURE
98.023
CYLINDER NO.
               MINOR
               COMp.
                     THAN H DATA CARDS.
MAJOR
COMP .

F-01363
.F-01364
r-01366
F-01367
F-01369
F-01370
F-01372
F-01374
(GRAMS CO
4.270
70.212
69.490
79. 190
9.724
19.228
27.490
33.870
                          (GRA^S N2
                             427.635
                             296.448
                             205.874
                             206.171
                             308.339
                             364.650
                             353.732
                             337.881
COMMENTS DATA:
CYLINDER NO
Q&IHttHHHHHHt
F-01363
F-01364
F-01366
F-01367
F-01369
F-01370
F-01372
F-01374
*
4}
SCOTT



SCOTT
SCOTT
SCOTT
SCOTT

6582



8582
B5H2
o582
H5*2
                  MS)
              115.H04
              215.915
              196.903
              196.591
               20.449
               93.592
               90.777
              136.893
(GKAMS)
543.439
512.363
402.777
402.762
388.788
458.242
444.509
474.774
MASS
RATIO
•t>««tt«ttti-ti-tt

0.009H864
0.0031751
0.0041^43
0.0053221
0.0257206
0.0500.^89
0.0721102
0.1031716
BLEND
CONC.
•»•» •»•»«•» •»•»•&
(PPM)
988.8.500
3175.788
4185.219
5323.184
25725.941
50099.020
72124.563
103191.375
                                  CYL.
                                 PRESS.
                                                                 (PSIA)
                                                                  1512.
                                                                  1283.
                                                                   964.
                                                                   999.
                                                                  1323.
                                                                  13n4.
                                                                  1334.
                                                                  1319.
                       PROCESSED:  08:45.00  KAY 14, 1974
                                 18

-------
MASS KATIO MAJOH  DILUTANT  CONCtNlKAT IQM PWF.SS'J^t' BLENDING  DATE
F-01374
r-01372
F- 01 370
F-01369
G-11832
G-11842
G-11871
G-11864
H-89471
F-01363
F-01367
F-01366
F-01364
H-89456'
G-11841
G-11833
G-11831
G- 11 849
G-11829
G-11863
G-11856
H-89474
G-11828
G-11873
H-89475
G-11848
G- 11 838
G-11840
G-11825
H-89469
H-89460
G-11845
G-11839
G-11854
G-11868
G-11850
G-11862
H-89462
G-11853
G-11866
G-11847
6-11858
H-89464
H-89476
G-11870
G-11867
H-89465
G-11851
G-11843
G-11872
,-11844
G- 11 837
H-89473
G-11846
G-11860

1.0317E-01
7.21 lOE-0?
5. OOd;>K-02
2.5721L-02
1.91 7-iE-02
1 .669f<
AIR
19
103191.374

50099. nPO
25725.941
19181.750
167U1.809
16638.902
16584.137
16207. S51
9888.500
5323.184
4185.219
3175.788
2815.347
2413.045
1836.925
1410.503
1227.580
9*9.817
901.215
705.462
522.192
462.176
256.333
192.006
126.660
104.014
90.B79
50.312
29.844
9.186
15.682
1 3.fc62
Il.fr91
8.fi35
6.768
5. (i 19
3.753
3.0^*5
2.453
1.968
1.6*3
1.075
1.025
O.S34
0.631
0.620
0,423
0.230
9472.020
8161. 9rt8
123d. 997
1212.553
464. lrtt>
430.960

1319.
1334.
13^4.
132J.
1230.
1494.
1505.
1534.
152b.
1512.
999.
964.
1283.
1595.
1547.
1512.
1565.
1516.
1424.
1443.
1538.
1447.
1365.
1526.
1389.
1475.
1388.
132d.
.1366.
1023.
105*.
1799.
1524.
1460.
1590.
1567.
1566.
1400.
1<*HO.
1537.
153V.
1490.
1279.
1120.
1076.
1092.
1584.
1118.
1543.
74d.
1435.
1035.
1639.
1023.
1247.
TP-101
05-11-74
05-11-74
05-11-74
05-11-74
05-1 1-74
12-10-73
01-16-74
01-16-74
01-16-74
05-11-74
05-11-74
05-11-74
05-11-74
08-25-73
04-13-73
04-13-73
04-13-73
04-13-73
04-13-73
11-01-73
04-13-73
11-01-73
11-05-73
03-02-73
08-25-73
08-25-73
11-01-73
08-25-73
11-01-73
08-25-73
08-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
09-25-73
02-22-7*
02-22-74
02-21-7*
09-25-73
02-21-74
02-21-74
03-02-73
03-02-73
03-02-73
08-28-73
10-01-73
03-02-73

Attachment No. 4

-------
6.2204F-04
G-11827
Ci-llB(S9
1-89470
M-89459
H-89466
H-89457
H-89480
G-11835
G-11857
H-89472
G-11852
G-11826

H-89458
2.H330E-04
1.1360F-OA
9.477^-05
6.7034F.-OS
3.717*»F>Ob
2.2«9<»0t>05
1.3^1<»E-05
9.bl87E-06
4.6B32E-06
1.6650E-OA  C3H8   N2
C3hd
C3nri
C3Hd
CJriM-
C3hd
C3rib
C3hfc
C3hb
C3Hb
C3H&
ft IK
A IK
AM
AM
AM
AM
AM
AM
AM
AM
40 /. 102 •
3.il .So4
2bv.fc35
le*S.?8H
107.778
99. ^0^
74.332
62.01M
43.HA3
24.324
1 b . 0 1 0
«. 777
6.228
J.064
770.
14 Ob.
I'^O.
1 o 0 -} .
741).
1229.
101*f.
101^.
106«.
1011.
1010.
1042.
14.^2.
1486.
03-02-73
03-M2-73
03-02- /.3
03-02-73
03-U2-/3
Oh-2o-73
11-29-73
03-02-73
10-01-73
10-01-73
11-29-73
10-01-73
10-01-73
10-01-73
105.791
1194.   08-28-73
          PROCESSED:   08:45.05  MAY 14.  1974
                     20
                                           TP-101
                                           Attachment No.

-------
   EPA    TEST   PROCEDURE
                                       Number
                                                 TP-102
                                                          Page
                        of  9
   SUBJECT

       Calibration of Gas Mixtures (Gas Analysis)
   Reference
       FR 85.075-23(a)  (4)
                                                          Data Form No.
   Responsible  Organization
       Correlation & Maintenance
                                                          Computer Program
                                                              CYLANAL
   Test Witness
       Requestor,
             /Review
             Quality Assurance
              Performance Interval
                 See Below
   Type of Test  Report
  	  Computer Print Out
                                                          Supersedes
                                                              New
   Report Distribution
  	Purchasing,  Correlation & Maintenance
                                                          Superseded by
   REMARKS/COMMENTS
         1.    Analysis of calibration gases are performed when  the  gases
              are received from a vendor,  when requested by  a contractor
              or manufacturer for correlation and traceability  reasons
              and when an in-house gas is  suspect for any reason.
                             ORIGINAL RELEASE APPROVALS
   Office
                Section
Signature
Date
                   Qnal
                             Mii^n^o
Administration
             Procurement
Jli
Branch
                   Supervisor
 Lab.  Branch
             Support Oper. Supv.
                                      REVISIONS
  Change
  Letter
              Description of Change
                                       "2T
        Approval
Date

-------
REVISIONS:


CALIBRATION OF GAS MIXTURES
TEST PROCEDURE
PROCEDURE NO.
TP-102
PAGE.2_OF .!__
1.0  PURPOSE

     To determine gas mixture concentrations by comparing them to known standards
     used as calibration gases, working gases and, in some cases, zero gases for
     the EPA laboratory, contractors, manufacturers.

2.0  TEST ARTICLE DESCRIPTION

     A gas blend or mixture blend of two or more gases under pressure in a cylinder
     or other suitable container.

3.0  REFERENCES

     3.1  Analytical instrument manuals

     3.2  "Handbook of Compressed Gases", Compressed Gas Associaton, Inc.,
          N.Y., N.Y., Reinhold Publishing Corp., Inc., 1966.

4.0  REQUIRED EQUIPMENT

     4.1  Primary gas standards, verified, gravimetric, or NBS cylinders.  Verified
          standards must be traceable to the EPA gravimetric standards by not more
          than one generation.  Zero gas, air or nitrogen as required.

     4.2  Analytical instruments with the following minimum specifications:

          Sensitivity:        Full scale for the concentration to be determined.

          Reproducibility:    1% of full scale, for successive identical samples.

          Stability:          Electronic stability of +1% per 24 hours.

          Response:           90% of scale in 0.5 seconds.

          Dectector Type:     CO, CO2 - NDIR:  HC - FID, NO - CHEMI.

     4.3  Sample handling system, manual or automatic, designed for a minimum hook
          up of 2 span gases, one zero gas and the gas to be analyzed.  The system
          need not be equipped with a sample pump unless required but should have
          line filters, flow meters and pressure gauges.  The materials of con-
          struction of the equipment prior to the instrument sample inlet should
          be of teflon, stainless steel and viton.  Use best judgment for the in-
          strument exhaust plumbing and equipment.

     4.4  Pressure regulators, dual stage, outlet pressure to be regulated between
          0-80 PSIG, inlet pressure rated at 4000 PSI with a gauge  0-3000 PSI.
          The regulator should be equipped with a purge port and safety relief
          port.  Regulators used for nitrogen oxide or any other corrosive gas
          should be of stainless steel construction only, the other gases require
          brass with teflon or viton seals.
                                        23

-------
REVISIONS^

CALIBRATION
TEST
OF GAS MIXTURES
PROCEDURE
PROCEDURE NO.
TP-102
PAOF 3 OF 9,,,
     NOTE;  Some regulators use a Buna N or other rubber type material  for
     construction of the diaphragm.  These should never be used for gas
     analysis for hydrocarbon or the zero gases.

     4.5  Recorder to match the output of the analytical instrument.

     4.6  Digital volt meter with the capability of reading the output to at least
          one significant figure (preferably two).

5.0  PRECAUTIONS

     5.1  Check work order for adequate information of the sample to be analyzed
          such as I.D. number, nominal concentration, sample pressure, components
          to be analyzed and type of analysis.

     5.2  Check the sample container for proper identification.  Check high pressure
          cylinder for date of last pressure test.  If longer than 5 years the
          cylinder should be returned to the vendor.

     5.3  Be sure that the analytical system and the regulator purge lines are
          properly vented to a hood or other air removal system.

     5.4  Excessively high flow rates or long analysis times should be avoided as
          this could use a large amount of span or sample gas.

6.0  VISUAL INSPECTION

     6.1  Examine sample container for damage.

     6.2  Check the container number against the work order for agreement.

     6.3  Check the analytical system for loose lines, dirty filters or missing
          parts.

7.0  TEST ARTICLE PREPARATION

     7.1  Attach a suitable pressure regulation device to the sample container.

     7.2  Secure the container and check all fittings for leaks using liquid
          detector such as "Snoop".

     7.3  Purge regulator and sample line through the venting system.

     7.4  Turn on instrument and allow to reach temperature and electronic
          stability.  Time will depend on instruments and previous history of use.

     7.5  Select two span gases, one should indicate a value above the maximum con-
          centration of the sample being evaluated and one below the minimal con-
          centration of the sample.  Neither span gas should exhibit values closer
          than ±10 percent of full scale of the sample concentration.

-------
REVISIONS:
                         CALIBRATION OF GAS MIXTURES

                           TEST     PROCEDURE
                                                  PROCEDURE NO.
                                                  	TP-102

                                                  PAGE_i_OF _2_
 8.0  TEST PROCEDURE

 Test Sequence

      101
               Test Description
Zero instrument using the same flow, pressure
and range as will  be used for the span and
sample gases.
NOTE:  Pressure should be measured closely
as possible to the detector inlet.
      102       Span  instrument using the highest  concentra-
                tion  standard at 95% of scale

      103       Switch to zero gas.  If instrument does not
                repeat zero, adjust and repeat 102.

      104       Repeat zero and span.

      105       Introduce second span gas and record deflection
                Repeat twice.

      106       Introduce sample gas at same flow  and pressure
                as  zero and span.  Repeat twice.   Reading should
                agree within ±0.2% of full scale.

      107       Introduce zero gas and both span gases.  Previous
                readings should agree within 0.2%  of full scale.
                If  not repeat procedure.

      108       Record data on form #102-01.

      109       If  the sample gas deflection does  not fall
                between the two points the gas may not be within
                the required tolerances.  Select another set of
                standards, repeat #106 and 107 and document results.
Data Output

0 ± 0.1
Reading
                                                      95.0 ± 0.2
                                                     0 ± 0.1
                                                     Average
                                                     Deflection
                                                     None

-------
REVISIONS:
                        CALIBRATION OF  GAS MIXTURES

                           TEST    PROCEDURE
PROCEDURE  NO.
    TP-102	
PAGE.5__OF
9.0  DATA INPUT

     Form No. 102-01 requires the following information:

     o    Data

     o    Analyzer train no.

     o    Mixture components

     o    Analyzer vendor

     o    Sample flow rate and pressure

     o    FID pressure,  air & fuel

     o    Operators initials

     o    Cylinder number analyzed

     o    Nominal concentration

     o    Analyzer setup data
          Low end concentration - meter deflection
          High end concentration - meter deflection
          Meter deflection of gas analyzed

     o    Comments:  Reference for standard gases used and zero gases.

10.0 DATA ANALYSIS

     10.1 Determine if low point and high point concentrations are adequate to
          determine the sample concentration.  Reliability of the data  is  a function
          of the separation of the two standards and the closeness to one  of the
          two standards.

     10.2 Determine that the  deflection for the sample gas is between (or  close to)
          the deflections for the bracketing standards.

     10.3 Confirm that operating parameters are within normal or recommended
          specifications.

     10.4 Check the calculated concentrations for apparent agreement with  deflection.

     10.5 Note comments for possible conflicts or indication of problems.

-------
REVISIONS:


CALIBRATION OF GAS MIXTURES
TEST PROCEDURE
PROCEDURE NO.
TP-102
PAGE-&-OF ?
11.0 DATA OUTPUT

     11.2 Data entered into cylinder inventory file.

     11.3 Data sent to person or company by division representative requesting
          the analysis.

12.0 ACCEPTANCE CRITERIA

     12.1 Instrument technician must determine that repetition of the zero gas
          is within ±0.1 deflection and that the span is within ±0.2 deflections.

     12.2 Deflection for the sample gas must be between the deflections for the
          two standards.

     12.3 The sample gas concentration determined must meet the blending specifi-
          cations requested from vendor.

13.0 QUALITY PROVISIONS

     13.1 Repetition of span and zero readings

     13.2 Repetition of sample readings

     13.3 Repetition of span and zero after sample analysis

     13.4 Data verification  (10.0)

     13.5 Acceptance criteria  (12.0)

-------
                                            GAS  BLEND ANALYSIS DATA
























DATE


-


-







xc
^
a:
*

S| 10
~
cr
:x






MIXTURE
COMP.

GAS








BAL




»l 20





















ANALYZER
VENDOR







35

|










SAMPLE
FLOW RATE



SCFH

30|






"H20



3S|

FID
PRESSURE-

AIR

«•!






FUEL









2i H^
-LJ 1—*
i_ *ZZ


»l





1
SO| js| . 40| *S| 70! «| • 10
1
CYLINDER NO.
ANALYZED
i
-




-




















-







-













1


-















-




-















—

NOMINAL
CONCENTRATION
(3)


-


-



















-











-




-







-









-
-
-
ANALYZER
LOW END
CONC. (1)
































._.

-
-4
-<

•-


































SETUP
METER
DEFL.

















—1












1-

DATA (NOTE)
HIGH END
CONC. (2)






-































-<



-


(




























PETER
DEFL.
















i
-t
H
-1



-
i-
:
~


-
-
-

(3)
METER
DEFL.
















..
•
'
-i




_








-



COMMENTS:











































































































































































1

































1




1
I



1
|





1








MM
                            30
30|
                                                                       '  S0|
_4SJ
TO!
10
NOTE:  Use verified, gravimetric, or NBS cylinders for analyzer setup values.
       Form 102-01

-------
200

-------
Section 200
CALIBRATION
        29

-------
EPA TEST
PROCEDURE Nl"ber ,
pp-201 Page _j 	 of _z 	
SUBJECT
CVS CALIBRATION PROCEDURE FOR POSITIVE DISPLACEMENT PUMP
Reference Federal Register, Vol. 38, No. 124, June 28, 1973, Uata fr°rm Mo-
Appendix III, 85.075-20
Responsible Organization
Correlation and Maintenance
Test Witness
Corr. and
201-01
Computer Program
SAQF:CALIBCVS
Performance Interval
Maint. Technician/Quality Assurance See Remarks
Type of Test Report
Computer Print-Out
Supersedes
New
Report Distribution Superseded by
Quality Assurance, Test Operations, Correlation & Maint.
REMARKS/ COMMENTS
1.0 CVS must be calibrated every 0, 50, 100, 200, 400, 800, etc., hours
of use or after major breakdown, cleaning and modification. The CVS
will also be calibrated as required to meet specific contract
requirements .
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt.
Lab. Branch
Lab. Branch



Change
Letter
Section
Quality Assurance
Test Ooer. Chief
Facilities Suooort Chief


REVISIONS
Description of Change

Signature





Date






Approval

Date

31

-------
REVISIONS:

CVS CALIBRATION PROCEDURES FOR
POSITIVE DISPLACEMENT PUMP
TEST PROCEDURE
PROCEDURE NO.
TP-201
PAftF 2 OP 7
1.0  PURPOSE

     To measure the various parameters which must be assessed to establish
     the flow rate of the constant volume sampler pump.  All the parameters
     related to the pump are simultaneously measured with the parameters
     related to a flowmeter which is connected in series with the pump.
     The calculated flow rate (ftvrev. @ pump inlet absolute pressure
     and temperature) can then be plotted versus a function that is the
     value of specific combinations of pump parameters.

2.0  TEST ARTICLE DESCRIPTION

     A constant volume sampler which meets requirements stated in Federal
     Register 85.075-20.

3.0  REFERENCES

     3.1  Federal Register^ Vol. 38, No. 124, June 28, 1973, 85.075-20,-
          Appendix III

     3.2  EPA, Ann Arbor, Preventive Maintenance Guidelines - Section I

4.0  REQUIRED EQUIPMENT

     The following equipment is required to perform the CVS calibration:

     4.1  LFE - Laminar Flow Element  (calibrated by manufacturer)

     4.2  Micromanometer  (see 7.3 for calibration check)

     4.3  Thermometer

     4.4  Timing mechanism

     4.5  u-tube Manometers

     4.6  Temperature Indicator with "J-Type" thermocouples  (see procedure #TP205
          for calibration)

     4.7  A variable flow restrictor with appropriate piping to connect
          CVS pump and LFE.

5.0  PRECAUTIONS

     5.1  Special care should be taken  in the initial set-up of the
          calibration equipment.  Leaks in the system or faulty calibration
          equipment will void the calibration.

-------
REVISIONS:
                       CVS CALIBRATION PROCEDURES FOR
                         POSITIVE DISPLACEMENT PUMP

                           TEST    PROCEDURE
PROCEDURE  NO.
    TP-201
5.2  The variable flow restrictor valve should be placed in the "open
     position"  at the  start of the calibration.  CAUTION:  never completely
     close the  valve while the pump is in operation; the motor may be damaged.

5.3  Temperature stability during the calibration is absolutely necessary.
     Air handling equipment must be shut off to avoid the normal 4°F oscil-
     lations.  Gradual temperature increases (2°F are acceptable as long
     as they occur over a period of several minutes.

5.4  Thermocouples must be checked for accuracy using a laboratory grade
     thermometer.

6.0  VISUAL INSPECTION

     6.1  Check LFE to CVS pump connections for loose fittings

     6.2  Check manometers for level placement.

     6.3  Check thermocouple  connections for tightness.

7.0  TEST ARTICLE PREPARATION

     7.1  Connect system as shown in Figure below.
                                             CVS Ca 1 ibrci t ion Configuration
              ETI
                         Figure 7-1

-------
REVISIONS:

CVS CALIBRATION PROCEDURES FOR
POSITIVE DISPLACEMENT PUMP
TEST PROCEDURE
PROCEDURE NO.
TP-201
PArtF 4 OF 7
7.2  Connect the LFE and variable flow restrictor to the CVS.  Carefully
     seal all connections to eliminate any leakage between the LFE
     and CVS pump.  NOTE;  Refer to previous LFE inlet Ap, a major drop
     may indicate a leak in connection.

7.3  Position the micromanometer and level the base using the adjustable
     feet provided.  Set the vertical and the vernier scales on zero
     and check the meniscus to assure that it is between the hairline
     reference marks.  If not, adjust the fluid at the rear of the
     case until the meniscus is zeroed.  Connect the LFE to the micromanometer
     and U-tube manometer with leaktight flexible tubing.  (See Figure 7-1.)

7.4  Attach the thermometer to the filter of the LFE so that the temperature
     of the air entering the LFE is indicated.

7.5  Check that the zero level of the U-tube manometers and adjust
     their scales accordingly.

7.6  Check that the CVS timer starts and stops when the counter power button
     is pushed.

7.7  Connect the thermocouples to the CVS at the pump inlet and outlet
     as shown in 7.1.  The fittings normally used for sampling, temperature,
     or sample dump connections may be used for thermocouples.

7.8  Start the CVS pump and open the U-tube manometer surge control
     valve 1/4 turn.  Check the fluid column surge; adjust the valve
     to insure the fluid will not oversurge (most surge control valves
     have been replaced by a 20 gauge hypodermic capillary fitting.)
     when switched from vacuum to pressure.  NOTE;  Two manometers
     may be used to measure these differentials simultaneously.

7.9  With the CVS pump running (20 minute warmup), adjust the micromanometer
     to the null position by cranking the vernier down.  Operate the
     revolution counter and timer to insure proper operation.

     7.9.1     Check the revolution counter by measuring revolutions
               of the pump using a strobotac and comparing the total
               revs, indicated on the counter for a 3-minute period.
                                    35

-------
REVISIONS:
CVS CALIBRATION  PROCEDURES FOR
 POSITIVE DISPLACEMENT PUMP

    TEST    PROCEDURE
                           PROCEDURE NO.
                            TP-201
8.0   TEST PROCEDURES

      The following data will be collected and recorded in order to calculate  the
      CVS calibration curve.
             Parameter
      Barmetric Pressure
        (Corrected)

      Ambient Temperature

      Air Temperature into LFE

      Pressure depression upstream
        of LFE

      Pressure drop across LFE
        meeting matrix

      Air temperature at CVS
        pump inlet

      Pressure depression at CVS
        pump inlet

      Specific Gravity of
       Manometer fluid

      Pressure differential at
        CVS pump outlet

      Air temperature at CVS
        pump outlet

      Pump revolutions during
        test period

      Elapsed time for test
        period
             Symbol    Units
 B


T

ETI


EPI


EDP


PTI
 "Hg



 Op


 Op



"H20



"H20



 Op
              PPI    "Fluid
             Sp.Gr.   "Fluid
              PPO    "Fluid
              PTO      °F
               N
        Revs.
                      Sees.
                        Tolerance
                       (accuracy of
                      data collected)
                                        +.01 "Hg


                                        ±.5 °F

                                        ±.1 °F
                                        ±.05  "H20
                                        ±.005  "H20
                                        + .5  °F
                         ±.05 "Fluid
                         +.05 "Fluid
                         ±.05 "Fluid
                         ±.5 °F
                                        ±0
                         +.05 Sees.
                                      36

-------
REVISIONS:
       CVS CALIBRATION PROCEDURES  FOR
         POSITIVE DISPLACEMENT PUMP

            TEST    PROCEDURE
PROCEDURE  NO.
   TP-201	
PAGE_§_OF ._L_
 Test Sequence

      101


      102

      103

      104

      105

      106

      107

      108

      109

      110

      110A

      111

      112

      113



      114


      115


      116
      117
            Test Description

Set variable restrictor valve  in  the wide
open position and run CVS  pump for  20 minutes

Start counter and timer

Read air temperature at CVS  outlet

Read pressure depression at  CVS pump inlet

Read pressure differential at  CVS pump outlet

Read ambient temperature

Read barometric pressure (corrected)

Read air temperature at CVS  inlet

Read pressure depression upstream of LFE

Read air temperature in LFE

ReadAP across the LFE matrix

Read pump revolutions for  test period

Record elapsed time for test period

Reset the restrictor valve to  a more re-
stricted condition.  A change  of about 4"H 0
is adequate to yield a minimum of six data points

Allow system to stabilize  for  a minimum of
3 minutes

Repeat steps 102 through 114 until  sufficient
data points have been established

Adjust temperature controller  and temperature
recorder on the CVS to indicate the proper
inlet temperature.  Disconnect the  micromanometer
and recheck zero setting

Disassemble the calibration  setup and recon-
nect all pipes and fittings  as used in NORMAL
CVS operation.  Check sample flow rates and
other indicators for normal  operation
    Data Output

         -0-
    PTO, °F
    PPI, "Fluid
    PPO, "Fluid
    V "Hg
    PTI, °F
    EDP, "
    ETI, °F
    EDP, "H2<

    N,  Revs.

    t,  sees.
         -0-
         -0-
                                       37

-------
REVISIONS:
CVS CALIBRATION PROCEDURES FOR
 POSITIVE DISPLACEMENT PUMP
                           TEST    PROCEDURE
PROCEDURE  NO.
                                                                     TP-201
                                        PAGE_L_OF
 9.0 DATA INPUT

     9.1  Complete data form 201-01
     9.2  Submit data sheet for analysis.

10.0 DATA ANALYSIS
     10.1 Analyze data using SAQF:CALIBCVS
          10.1.1  These are linear fits of VQ vs. X0 and RPM vs AP.

11.0 DATA OUTPUT

     11.1 Printed computer output
     11.2 CVS coefficients for storage in Instrument Data File.

12.0 ACCEPTANCE CRITERIA

     12.1 Verify new curve against previous curve and tracer gas readings
          previously obtained.

     12.2 All VQ measured values must lie within ±0.50% of the calculated V0
          values.  All RPM measured speeds must be within +0.25% of the
          calculated RPM values.

     12.3 Check and verify that the V-o vs Xo intercept is approximately
          350 ft3/rev and the RPM vs AP intercept is related to the
          synchronous speed of the blower motor.

13.0 QUALITY PROVISIONS

     13.1 An excessive shift from old curve to new curve may constitute an
          invalid test, therefore an investigation of cause should be
          implemented.

     13.2 Corrective action must be implemented if malfunctions are found and
          the procedure must be repeated.
                                       38

-------
                                    CVS CM, Hi NATION DATA SIlIiET








































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                            15J
                                    3C|
50|
       55 1
•ol
                    65
                                                                                                        SO
VD
          *NOTE:   Indicate  manometer  units
                   and fluid specific  gravity
                   on card one.
      INITS:   IN
               CM
               MM
                    Inches
                    Centimeters
                    Millimeters
   .Form 2.01-01

-------
                           CVS  FLO-' CALIBRATION'
                                                          TP-201
                                                          Attachment No.
                                *   CvS-O^C *
LAMINAR Fl-E^ENT:  Y72291R
     CVS  VFA'OOP:  AMI
     PUMP  RANG*-" :  300 CFM
                                                      ON DATE"
                                            EFKFCTIV7 TF.ST »
                                           CVS
                                                 07-13-74

                                                 1080.9
      MANOMFTF.P SPECIFICATIONS:
            LAM I hi AW. H.E^ENT:  IN.  OF   1.00
                   CVS PUMP:  IN.  OF   1.75
                             SPECIFIC
                             SPECIFIC
                                              GRAVITY
                                              GRAVITY
FLUIO
FLUID
MEASURED  DATA:
 AMBIENT
      FLEMENT
                                       cvs PUMP
                        «•»•&««• U •»«••» if «••»•»<>••»••«• O «• •U--M--& «••»•!>•» •»••»•» <• -i* «•«••»•» •»*•(}•
 8ARO    T     T
            (IN)
29.21  82.0  Q3.4
29.21  83.0  83.4
29.21  83.0  83.5
29.21  83.0  83.5
29.21  83.0  83.6
29.21  83.0  H3.8
29.20  83.0  84.0

CALCULATED  DATA:
P
(IN)
4 . 8S
4.75
4.65
4.55
4.50
4.45
4.35
DELTA

7.
7.
7.
7.
7.
7.
7.
P
594
510
414
303
221
11H
046
T
(IN)
H 0 . 0
ril . 0
r 1 .0
M .0
bO.O
eo.o
eo.o

(
17
19
21
23
25
27
29
P
I N )
.70
.30
.30
. 35
.10
.40
.00
T
(OUT)
o.o
0.0
0.0
0 . 0
0.0
0.0
0.0
P
(OUT)
lc- .
lf>.
18.
1^ .
1 P .
17.
17.
40
00
70
35
10
75
55
REV
COUNTS
62U9.
61rt7 .
6516.
6278.
6138.
6213.
6125.
TIME
(SECS)
257
253
267
257
252
255
252
.30
.30
.20
.60
.20
.70
.40


.
.
.
.
.
.
.

X
000265
000270
000276
000282
000288
000295
000300
CF/PEV
ACTUAL
0.2902
0.2901
0.2897
0.2886
0.2877
0.2872
0.2870
CF/PEV
C4LC
0.2903
0.289?
0.2891
0.2*85
0.?879
0.2872
0.2866

CALC/ACT
1 . OOOJ
0 , 9 •>•'•*   1974

-------
EPA TEST
SUBJECT
DYNAMOMETER
PROCEDURE NU'
CALIBRATION
TP-202 paae ! Qf 9

Reference Federal Register, Vol. 38, No. 124, June 28, 1973 Data Form No.
Appendix II , 85. 075-15 (d)
Responsible Organization
Correlation and Maintenance
709-1
Computer Program
DYNAHP
Test Witness /Review Performance Interval
Corr. & Maint. Technician, Quality Assurance Monthly
Type of Test Report
Computer Print-Out
Supersedes
New
Report Distribution Superseded by
Quality Assurance, Test Operations, Support Services, file
REMARKS/ COMMENTS
NOTE: This procedure is in the revision phase by EPA, Ann Arbor. The
final version will reflect new changes.
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Operations
Lab Operations


Section
Quality Assurance
Chief
Support Services Chief


Signature





Date





REVISIONS
Change
Letter
Description of Change
Approval
1,, - 	 - - ,
Date


-------
REVISIONS:

DYNAMOMETER CALIBRATION
TEST
PROCEDURE
PROCEDURE NO.
TP-202
PAGF 2 OF 9
1.0  PURPOSE

     The purpose of the dynamometer calibration procedure is to insure that
     the indicated speed and the indicated absorbed power (torque) are correct
     and to determine the frictional loss characteristics of the dynamometer.

2.0  TEST ARTICLE DESCRIPTION

     2.1  A direct drive chassis dynamometer, having the capabilities described in
          Federal Register 85.075-15.

     2.2  Speed and torque (hp @ 50mph) meters and controls

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 124, June 28, 1973 - Appendix II

     3.2  EPA, Ann Arbor, Preventive Maintenance Guidelines, Section III.

     3.3  SAE XJ1094 "Constant Volume Sampler System for Exhaust Emission
          Measurement," Section 3.7

4.0  REQUIRED EQUIPMENT

     4.1  Test vehicle

     4.2  Stroboscopic tachometer or electronic RPM counter (see manufacturer's
          manual for calibration procedure)

     4.3  Adjustable DC power supply, upper value of at least 8 volts DC

     4.4  Weight stand, Clayton

     4.5  Weights, 35 pounds and 10 pounds

     4.6  Tachometer generator assembly, Clayton

     4.7  Varian 614A, strip chart recorder  (see procedure #204 for calibration
          procedure)

     4.8  Stopwatch or electric timer  (±.1 sec.)

5.0  PRECAUTIONS

     5.1  Inflate the rear tires to 45 psi to protect against blow-outs and to
          equalize the contact (especially important with front-wheel drive
          and radials)

     5.2  Align vehicle on dynamometer.  (Drive vehicle on to the dyno, with
          vehicle perpendicular to the rolls, insuring that the front wheels
          are centered to prevent the rear wheels from sliding off the rolls.)

-------
REVISIONS:

DYNAMOMETER CALIBRATION
TEST
PROCEDURE
PROCEDURE NO.
TP-202
PAftF 3 OF 9
     5.3  Operate vehicle cooling fan within 12 inches of vehicle radiator.

     5.4  Vent vehicle exhaust.

6.0  VISUAL INSPECTION

     6.1  Check equipment set-up, (see sec.  7.0 and 8.0 for set-up
          instructions.


7.0  TEST ARTICLE PREPARATION

     NOTE:  Prior to calibration assure that the dynamometer is warmed up in
            accordance with procedure #TP-604

     7.1  Speed Meter Calibration

          7.1.1     Adjust mechanical zero of the speed meter with rolls stopped.

          7.1.2     Place range switch to "LO" position.

          7.1.3     Record dynamometer Serial Number.

          7.1.4     Place vehicle on dynamometer and tie it down.

          7.1.5     Engage flywheels for 4,000 pounds inertia.

          7.1.6     Check index on the end of front roll for visibility.

          7.1.7     Precondition the dynamometer by operating vehicle at 30 mph
                    for 15 minutes.

          7.1.8     Warm up strobotac and calibrate strobotac according to manu-
                    facturer's specifications.

     7.2  Power Meter Calibration

          7.2.1     All calibration steps take place with dynamometer rolls in
                    stationary position.

          7.2.2     Disconnect tachometer leads from torque bridge terminals.

          7.2.3     Attach variable voltage power supply to the torque bridge
                    terminals.

          7.2.4     Adjust meter to zero with power supply off.

-------
REVISIONS:
                            DYNAMOMETER CALIBRATION
                          TEST    PROCEDURE
PROCEDURE NO.
	TP-202

PAGE_i_OF JL-
      7.3  Determination of Actual Power Absorption

           7.3.1     Inspect the dynamometer  and service according to manufacturer's
                     recommended procedure.

           7.3.2     Install tachometer generator on the dynamometer frame.  Line
                     up the tach generator pulley with the shaft adaptor pulley
                     on the front roll.  Insure that the center to center pulley
                     distance is the same as  the factory installed tach generator.

           7.3.3     Attach front roll tachometer generator electrical leads to
                     Varian chart recorder.

           7.3.4     Drive vehicle on dynamometer and attach vehicle restraint
                     system.

           7.3.5     Disengage roll brakes.

           7.3.6     Adjust recorder zero.

-------
REVISIONS:

DYNAMOMETER CALIBRATION
TEST
PROCEDURE
PROCEDURE NO.
TP-202
pArtF 5 OF 9
8.0  TEST PROCEDURE

     The dynamometer calibration is actually separated into three separate
     procedures.  Therefore, the steps listed below are listed in three
     sections.  Section I pertains to speed meter calibration; Section II
     covers power meter calibration and Section III outlines the determination
     of actual power absorption.
Test Sequence
     101
     102
     103
     104
     105
     106
Test Sequence

     201
          SECTION I.  SPEED METER CALIBRATION

                    Test Description

Operate vehicle at front roll speed of 1,800 rpm
Set strobe tach at 1,800 rpm flash rate and aim
at the front roll index mark.  Adjust vehicle speed
to hold the mark steady at 1,800 rpm.

When the front roll is steady at 1,800 check the
speed meter display.  ECE-50 with DD-VIF will
indicate 46.3 mph if speed meter is calibrated
correctly.

If the meter indicates other than 46.3 mph, adjust
the speed meter calibration pot in the readout
instrument assembly, until speed meter indicates
correct speed.

Repeat steps 101 through 103.  If readings will not
repeat within ±0.5 mph without readjustment a malfunc-
tion must be reported.  Necessary maintenance should
be performed before continuing with calibration.

Reduce roll speed to 900 rpm and hold steady.  The
speed indicated on the meter should be 23.15 (±0.5)
mph.  Any nonlinearity will be reported and cor-
rected.  (Perform necessary maintenance before
continuing procedure.)

When calibration is complete, attach calibration
sticker to the back of speed meter.

        SECTION II.  POWER METER CALIBRATION (TORQUE)

                      Test Description

Turn on power supply and adjust voltage to display
46.3 mph on the speed meter.
Data Output
Data Output

-------
REVISIONS:
                              DYNAMOMETER CALIBRATION
                           TEST     PROCEDURE
                                                 PROCEDURE  NO.
                                                      TP-202
  Test  Sequence
       202
       203
                    Test Description

Install the weight  stand  (Arbor) on the Torque
Arm.  Tighten the attaching bolt.

Level the torque arm by turning ball joints in or
out of the load cell.
Data Output
       204       Place  (one) 35 Ib. weight and (one)  10 Ib.
                weight totaling 50 Ibs.  on the  weight
                stand  (Arbor wt. stand = 5 Ibs.).  Torque/
                Power meter should show 50 ft.  Ibs.  of torque.
                If meter does not show proper value, adjust
                the meter using the Torque Meter Calibration
                pot.

       205       Repeat Step 204 substituting weights:
                 (1) 10 Ib. weight = 15 ft. Ibs.  torque and
                the weight stand itself 5 Ibs = 5  ft. Ibs.
                torque on meter.  The nonadjusted  torque
                readings should agree within ±1 ft.  Ib. of
                torque.  If meter does not agree within limits
                without readjustment, a malfunction  should be
                reported.

       206       After completing the calibration with no mal-
                functions, a calibration sticker should be
                placed on the meter.

             SECTION III.  ACTUAL POWER ABSORPTION  CALIBRATION
  Test Sequence
       301
                 Test Description

Accelerate vehicle  to 60 mph and hold steady.
Calibrate the chart recorder at 60 mph full
scale.
       302       Check the calibration of chart  at  55,  50, and
                45 mph.  Insure that 55 and 45  mph points are
                easily identified.

       303       Bring the vehicle to a complete stop and
                re-zero the recorder.
                                                      50  ft.  Ibs.
                                                      15  ft. Ibs.
                                                      5 ft. Ibs.
Data Output
                                                      55  = 	divis.
                                                      45  =   divis.

-------
REVISIONS:
                             DYNAMOMETER CALIBRATION
                           TEST    PROCEDURE
                                                  PROCEDURE NO.
                                                      TP-202	

                                                  PAGEJL-Of _L_
Test Sequence
      304
              Test Description

Measure the recorder chart speed with a stop-
watch or other timing mechanism.  This should
be repeated at least 3 times  for an accurate
measurement of the distance the paper travels
in one (1) minute.
NOTE:     Alternate method of measuring elapsed
          time:  Direct measurement of time
          elapsed between  55  mph and 45 mph can
          be accomplished  by  starting electronic
          timer at 55 mph  and stopping at 45 mph.
          This method will eliminate interpolation
          of chart method.
                                                 Data Output

                                                 Chart Speed
                                                 (inches/mins)
      305
      306
Set dynamometer inertia at  1,500  Ibs.
that rolls are stationary.)
                                       (Insure
Accelerate vehicle to 50 mph and hold steady.
Set the Hp (torque)  to lowest obtainable
value.
                                                      Hp
     307
     308
     309
     310



     311

     312


     313
                                                 Time sees.,
                                                 IHP
Increase speed to 60 mph and use a winch or
alternate means to pull  vehicle off the front
drive roll.   Release accelerator and allow
vehicle to decel (caution:  insure rear
wheels are completely clear of drive roll) .

Measure and record the elapsed time it takes
the front roll to slow from 55 mph to 45 mph.

Loosen the winch and allow vehicle's rear
wheels to contact the front roll.  Match the
front roll speed and vehicle speed as closely
as possible to prevent tire damage.
Repeat Steps 307-309 so  that two measurements     Elapsed Time
are taken at even 500 Ib.  increments of inertia   IHP
starting at 1,500 Ibs. and ending with 5,500 Ibs.

Stop vehicle and check recorder zero.

Operate vehicle at 50 mph  and set Hp at 8.0
indicated Hp.
Repeat Steps 307-309  so  that two readings are
taken at each inertia setting, at 8.0 indicated
Hp.
                                                                Elapsed Time
     314
Repeat Step 311.

-------
REVISIONS:
                            DYNAMOMETER CALIBRATION
                          TEST    PROCEDURE
                                                PROCEDURE  NO.
                                                   TP-202

                                                PAGE.8_OF  9
Test Sequence
     315
     316
     317
            Test Description

At a steady 50 mph reset Hp to 14.0  indicated
horsepower.

Repeat Steps 307-309 in order that two readings
are taken at each inertia at 14.0 indicated
horsepower.

Remove vehicle from dyno and restore all equip-
ment to normal operating conditions.
Data Output
Elapsed Time

-------
REVISIONS:
                             DYNAMOMETER CALIBRATION
                           TEST    PROCEDURE
PROCEDURE  NO.
                                                                     TP-202
PAGE_£.OF .9.
 9.0 DATA INPUT

     9.1  Complete form No.  202-01.  Submit the form and recorder charts to the
          Data Branch for analysis

     9.2  Transfer information to data cards for computer input.

10.0 DATA ANALYSIS

     10.1 If a chart speed of 6 inches/minute or faster, elapsed time measurements
          for coastdowns are made from the chart.  To make this measurement, the
          distance between the point the trace crosses the 55 mph speed and the
          point the trace crosses the 45 mph speed is measured to the nearest
          0.01 inch.  This distance is then divided by the chart speed.

     10.2 A manual curve plot of actual power versus indicated absorber power
          (pHp vs pind^  is made f°r each inertia setting.

     10.3 Final analysis is made by computer program DYNAHP.

11.0 DATA OUTPUT

     11.1 Computer print-out of inertia weight (1,500 to 5,500 Ibs.)  and
     indicated horspower per Federal Register requirements shown in
     paragraph 85.075-15(d).

12.0 ACCEPTANCE CRITERIA

     12.1 New calibration curve should be within ±1/2 horsepower
          of previous calibration (SAE XJ 1094)

     12.2 Compare graph plots of calibration results with the computer output
          to insure the data is accurate.

13.0 QUALITY PROVISIONS

     13.1 If any malfunctions are reported for speed meter or torque meters,
          insure the proper corrective maintenance is performed and a
          repeat calibration has been accomplished.

     13.2 If calibration does not agree with 12.1 above, reject calibration.

     13.3 Perform necessary corrective maintenance or action and repeat the
          calibration.

-------
                                DYNAMOMETER CALIBRATION
DYNO
NO.






DATE
MO DY
i

5|
CARD
NO,
2
3
4
5
6
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8
9
10
11
12
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17
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5
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PROGRAM: r

75 1 SO
YNAHP
FORM 202-01

-------
  03 02-04-74    18. 8  HP  1800
PKUCESSEO:  17:05.48   Ft*
                                  =  ^b.3  MPH
                                                      Attachment No.
                               1974  -

WT.
1750.
2000.
2250.
2500.
2750.
3000.
3500.
4000.
4500.
5000.
5500.
5500.
ACT.
HP
7.7
8.3
8.8
9.4
9.9
10.3
11.2
12.0
12.7
13.4
13.9
14.4
I NO.
HP
4.9
4.9
5.2
5.7
6.2
6.5
7.0
8.0
d.2
8.9
8.9
9.3
«'ITH
ft/C
5.5
5.6
6.0
6.5
7.1
7.4
7.9
9.1
9.3
10.1
10.1
10.5
NOTE:  LAST 5500 VALUE  IS F0«  «TS  ABOVE  5751*
    INPUT VALUES
  03 02-04-74   18.6 HP  1600  RPM  =  46.3
WT
1750.
20UO.
2500.
3000.
3500.
4000.
4500.
5000.
b500.
1750.
2000-
2500.
3000.
J500.
4000.
451)0.
5000.
5500.
1750.
2000.
25 'JO.
3000.
3500.
4000.
4500.
5000.
5500.
T
16.00
17.00
20.80
25.00
27.70
32,70
35.10
3*. 10
40. bO
9.30
9.90
12.40
15.00
17.00
2 0 . 0 G
21. 70
24.40
25. bO
5.70
6.40
8.00
9.70
10.90
13.00
14.20
16.00
16.90
I NO. HP
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
4.0
8.0
8.0
8.0
8.0
8.0
o.O
b.O
8.0
8.U
14,0
14.0
14.0
14.0
14.0
14.0
14.0
1^.0
14.0
ACT. HP
b.6
7.1
7.3
7.3
7.7
7.4
7.8
o.O
«.2
11.4
12.3
12.2
12.1
J2.b
12.1
12.6
12.4
13.0
18.6
19.0
19.0
18.8
19.5
18,7
19.2
19.0
19.8
C&LC.
4.0
3.9
3.9
3.9
4.0
3.9
3.9
4.0
3.9
8.0
8.2
P. 2
H.I
8.1
>.l
8.1
fc.O
8. 1
14.0
13.9
13.9
13.9
14.0
)3.9
13.9
14.0
14.0

-------
EPA TEST
Number
PROCEDURE TP-203
Page l of 6
SUBJECT
GAS ANALYZER CALIBRATION CURVE GENERATION
Reference FEDERAL REGISTER, VOL. 38 NO. 209,
Oct. 31. 1973 - 85.075-23
Responsible Organization
CORRELATION/MAINTENANCE
Test Witness /Review
QUALITY ASSURANCE
Type of Test Report
COMPUTER PRINT-OUT (DEFLECTION VS CONCENTRATION)
Report Distribution QUALITY ASSURANCE, TEST OPERATIONS,
CORRELATION AND MAINTENANCE
Data Form No.
203-01
Computer Program
SAQF : CURVEALL
Performance Interval
See Comments
Supersedes
New
Superseded by
REMARKS/ COMMENTS
1.0 Calibration should be performed every 30 days, after any maintenance
requiring re-alignment or when called for specifically by contract
requirement .
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Branch
Lab Branch



Change
Letter
Section Signature
Quality Assurance
Chief


Support Services Chief


Date





REVISIONS
Description of Change Approval

Date

53

-------
REVISIONS:


ANALYZER CALIBRATION
TEST
PROCEDURE
PROCEDURE NO.
TP-203
PAGE-2L-OF ,fi
1.0  PURPOSE

     Measurement of exhaust components requires that the deflections obtained
     during the analysis be converted to concentrations as accurately as
     possible.  This document describes the procedure to be used to construct
     calibration curves for the instruments which measure hydrocarbons,
     oxides of nitrogen, carbon dioxide and carbon monoxide.

2.0  TEST ARTICLE DESCRIPTION

     The instruments being calibrated are mounted in a console with provisions
     for: analysis of the exhaust sample; recording the instrument outputs; and
     suitable gas supplies for spanning and zeroing the instruments.

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 209, Oct. 31, 1973 - 85.075-23

     3.2  SAE XJ1094, "Constant Volume Sampler System for Exhaust Emission
          Measurement," Section 4.  (Proposed)

     3.3  Operators Manuals for In Use Analyzers

4.0  REQUIRED EQUIPMENT

     4.1  Exhaust gas analysis console, equipped with the following instruments:

          4.1.1     Hydrocarbons by flame ionization
                    Beckman Model 400 or equivalent

          4.1.2     Carbon monoixde by non-dispersive infrared (NDIR)
                    Bendix Model 8501B or equivalent

          4.1.3     Carbon dioxide by non-dispersive infrared (NDIR)
                    MSA Model 202 or Beckman Model 315B or equivalent

          4.1.4     Oxides of nitrogen by chemiluminescence
                    Teco Model 10A or equivalent

          4.1.5     Flow controls for selecting and monitoring the gases

     4.2  Zero gas meeting the requirements specified in FR 85.075-23  (a)(2).

     4.3  Calibration (standard) gas mixtures traceable to NBS and/or EPA
          primary standards.

     4.4  Chart recorders capable of 0-100 deflections with accuracy of
          ±1 percent, and a readability of ±1 percent.
                                        55

-------
REVISIONS:
                              ANALYZER CALIBRATION
                           TEST    PROCEDURE
PROCEDURE  NO.
    TP-203	

PAGEJ—OF 6	
      4.5  Read-out device in percent of  scale.

               o    Computer interface
               o    DVM
               o    Meter

 5.0  PRECAUTIONS

      5.1  Safety - Reference safety manual "Safe Handling of Compressed  Gases."

      5.2  Meter chart reading,  D.V.M. or other output devices should have  a
          valid calibration tag.

      5.3  Check that the proper set of standards are used for the particular
          range being calibrated as specified by Quality Assurance.

 6.0  VISUAL  INSPECTION

      6.1  Verify that the instrument serial number is correct for the sample
          train.

      6.2  Check instrument gain settings against those in the instrument
          log book.

      6.3  Check instrument response time and noise level.

 7.0  TEST ARTICLE PREPARATION

      7.1  Check calibration gas mixture  for proper cylinder and regulation
          pressures.

      7.2  Special checks; Converter efficiency test procedure No.  303.

      7.3  Adjust analyzers to optimum performance.

          7.3.1     Reference analyzer operation manuals

-------
REVISIONS:
                               ANALYZER CALIBRATION
                           TEST    PROCEDURE
                                                 PROCEDURE  NO.
                                                      TP-203

                                                 PAGE JL.OF JL
  8.0  TEST PROCEDURE

       The calibration curve  is constructed from the data collected as  a  result of
       performing the following sequence of steps:
  Test Sequence
       101
       102
       103

       104


       105

       106
       107
       108
       109
       110
               Test Description

Zero the instrument using  zero gas flowing at the
same rate used for span  and sample.  The HC instru-
ment must be zeroed with air, others with nitrogen
or air.

Select desired range,  introduce calibration gas with
highest concentration  for  that range.  Adjust output
to reading obtained in previously monthly calibration
or determine theoretical percent of scale (TPS) by
              Data Output

              ZERO DEFL.
              RANGE
                           Cylinder Cone.
                           X100
TPS
           Range Cone.

TPS should never be  greater than 99 percent.

Introduce zero gas.   If  not zero, adjust.

Introduce highest span gas


Repeat 103

When steps 103 and 104 can be repeated without
adjustment, go on to 107.  If not within a
reasonable period of time, follow instrument
diagnostic and maintenance procedures. Ref. 3.3.

Introduce each successively lower span gas until
zero is repeated.

Introduce each successively higher span gas
until highest reading is obtained.

Repeat steps 107 and 108 until all readings agree
within ±0.25%.  If not possible, perform instrument
diagnostic and maintenance procedures.  Ref. 3.3.

Record average of all readings except zero on data
form # 203-01
              ZERO  DEFL.

            CONCENTRATION/
              DEFLECTION
              CONG  &  DEFL.
              CONG  &  DEFL.
              DEFLECTIONS
                                       57

-------
REVISIONS:
                              ANALYZER CALIBRATION
                          TEST    PROCEDURE
                                               PROCEDURE NO.
                                                    TP-203
  Test  Sequence
       111
              Test Description

Record the following information on the data sheet
date,  analyzer, train no., gas analyzer,  range no.,
full scale concentration, analyzer vendor, NDIR
cell length, units, flow  rate set point,  FID pres-
sures,  gain setting, recorder type used,  operators
initials, also cylinder numbers, and concentrations.
Data Output

   SEE
DATA SHEET

-------
REVISIONS:


ANALYZER CALIBRATION
TEST PROCEDURE
PROCEDURE NO.
TP-203
PAfiF 6 OF 6

9.0  DATA INPUT

     9.1  Complete form # 203-01.

     9.2  Submit the form to the Data Branch for processing.

10.0 DATA ANALYSIS

     10.1 Process data using "SAQF: CURVEALL"

11.0 DATA OUTPUT

     11.1 Computer print of "Curveall Super Version" Recorder Deflection vs.
          Concentration.

12.0 ACCEPTANCE CRITERIA

     12.1 Check for linearity of NOx and HC curves.

     12.2 Insure that all calibration points fit within ±2% of the point value.

     12.3 Insure that no major curve shift was indicated from last calibration.

13.0 QUALITY PROVISIONS

     13.1 if data does not follow  "Acceptance Criteria", reject calibration and
          institute corrective action.

     13.2 If data is acceptable and curve update is desired, check the
          appropriate space on the Curveall Verification sheet and return
          it to the Data Branch.

     13.3 If data was unacceptable, upon completion of required corrective
          action, institute recalibration.
                                         59

-------
                                               ANALYZER CALIBRATION
                                               .CURVE GENERATION DATA
















DATE


-




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-








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O _J
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COMMENTS:
CYLINDER
, NUMBER

























-














•
--










-



















-








-



-


-



-


-








-



CYLINDER
,3 cone.
-
















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i
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-



                                           SYMBOLS AND ABBREVIATIONS
                                           GASES - CaHs, CO, C02, NOX, CH4

                                           CELL LENGTH UNITS - IN, CM

                                           RECORDER TYPE - TI (Texas .Instr.),  HW (Honeywell),  LN  (Leeds  &  Northrup),
                                             DVM (Digital Voltmeter), MIS (Other).
PROGRAM:  SAQF:CURVEALL.
10-30-73
RANGE NO. DESIGNATIONS

HC, co, nox (PPM)

  01 - 0 -   10
  02 - 0 -   25
  03 - 0 -   50
  04 - 0 -  100
  05 - 0 -  250
  06 - 0 -  500
  07 - 0 - 1000
  08 - 0 - 2500
  09 - 0 - 500&
CO, C02 (%)

01 - 0 -  1.0%
02 - 0 -  2.5%
03 - 0 -  5.0%
04 - 0 - 10.0%
05 - 0 - 15.0%
HEXANE NDIR

01 - 0 -  1000 PPM HEX
02 - 0 - 10000 PPM HEX
         FORM 203-01

-------
*»» CURVEALL SUPER VERSION »**
CALIBRATION DATE
ANALYZER TRAIN
GAS ANALYZED
RANGE NUMBER
FULL SCALE CCNC.
ANALYZER VENDOR
NDIR CELL LENGTH
SAMPLE FLOWRATE
MONITOR SET POINT
FID AIR PRESSURE
FID FUEL PRESSURE
FID SAKP PRESSURE
ZERO GAIN
SPAN GAIN
RECORDER TYPE
OPEHATOR'S INIT.
COMMENTS




EQUATION:
«»•»»«««•»
ON
H
CO = X /


COEFFICIENTS:
•Q-«e»4««ee»»»

(A) 3
fb) -3
(C) 3
6h66666666
5000.0 1111 66 66
'BECKMAN 11 66
0.0 11 66
0.0 SCFH 11 66666666666
13.0 "iH20 11 666666666666
0.0 PSI 11 f>6 66
0.0 PSI 11 66 66
0.0 PSI 11 66 66
0.0 1111111111 666666666666
0.0 1111111111 6666666666
DVM
RR
0-5000 PPM CO






2 3
( A + B°X * C*X * 0»X )





.3993E-02
.1195E-04
.2324E-06
.7609E-U8


CYLINDER RECORDER CO CONCENTRATIONS % POINT
NUMBER DEFLECTION CYLINDER CALCULATED DEVIATION

(X) (Y)
A2827 26.90 976.172 974.712 -0.15
MH1594
+0.^0 1576. 6o9 15W4.002 0.47
A8442 56.10 23V6.665 2381.^62 -0.64
As397 71.60 32cs3.272 33C2.510 0.59
A6146 83.90 4170.984 4158.727 -0.29
A9172 95.30 5182.027 5184.663 0.06


AVERAGE PERCENT OF POINT DEVIATION: 0.37












»<*»PROCESSED: 15:43 MAY 2c» 1975

»»<*LOGGEO ON LINE: 389
'>*>>TO: )<-,/,i/09 05-20-75

0.0 0.0
0.5 14.78
1.0 29.69
1.5 44.73
2.0 59.91
2.5 75.23
3.0 90.67
3.5 106.25
4.0 121.97
4.5 137.81

5.0 153.79
5.5 169.90
6.0 186.14
6.5 202.51
7.0 21s>. 01
7.5 235.64
6.0 252.40
6.5 269.29
9.0 286.31
9.5 303.45

10.0 320.73
10.5 338.12 '
11.0 355.65
11.5 373.30
12.0 391.07
12. b 406.97
13.0 426.99
13.5 445.14
14.0 463.41
14.5 481.60
15.0 500.30
15.5 nltf.93
16.0 537.68
10.5 556.55
17.0 575 .54
17.5 594.64
ld.0 613.96
lb.5 633.20
19.0 652.65
19.5 672.21

20.0 691.89
20.5 711.69
21.0 731.59
21.5 751.61
22.0 771.73
22.5 791.97
23.0 812.32
23.5 832.78
24.0 .153.34
24.5 674.01


25.0 894.79
25.5 915.68
26.0 936.67
26.5 957.76
27.0 976.96
27.5 1000.26
28.0 1021.67
28.5 1043.18
29.0 1064.78
29.5 1086.50

30.0 1108.31
30,5 1130.22
31.0 1152.23
31.5 1174.34
32*0 1196.54
32*5 1218.85
'33*0 1241.25
33.5 1263.75
34.0 1286.35
34*5 1309.04

35.0 1331.83
35.5 1354.72
36*0 1377.70
36.5 1400.77
37.0 1423.94
37*5 1447.21
38.0 1470.57
38.5 1494.02
39*0 1517.57
39*5 1541.21
40.0 1564.95
40*5 1588.78
41.0 1612.70
41.-S 1636.72
42.0 1660.83
42*5 1665.04
<+3.0 1709.34
43.5 1733.73
44.0 1758.22
44.5 1782.81

45.0 1807.49
45.5 1632.27
46.0 1857.15
46.5 1882.12
47,0 1907.19
47.5 1932.35
48.0 1957.62
48.5 1982.99
49.0 2008.45
49.5 2034.02


50.0 2059.69
50.5 2085.46
51.0 2111.34
51.5 2137.32
52.0 2163.41
52.5 2189.60
53.0 2215.90
53.5 2242.32
54.0 2268.84
54.5 2295.47

55.0 2322.22
55.5 2349.09
56.0 2376.07
56.5 2403.17
57.0 2430.39
57.5 2457.74
58.0 2485.21
58.5 2512.80
59.0 2540.52
59.5 2568.38

60.0 2596.36
60.5 2624.49
61.0 2652.75
61.5 2681.15
62.0 2709.69
62.5 2738.37
63.0 2767.21
63.5 2796.20
64.0 2825.34
64.5 2854.64
65.0 2384.09
65.5 2913.71
66.0 2943.50
66.5 2973.46
67.0 3003.59
67.5 3033.91
68.0 3064.40
68.5 3095.07
69.0 3125.94
69.5 3157.00

70.0 3188.26
70.5 3219.73
71. U 3251.40
71.5 3263.28
72.0 ' 3315.38
72.5 3347.70
73.0 3380.24
73.5 3413,02
74.0 3446.04
74.5 3479.31

75.0 3512.82
75.5 3546.59
76.0 3580.62
76.5 3614.92
77.0 3649.49
77.5 3684.35
78.0 3719.49
78.5 3754.93
79.0 3790.68
79.5 3826.73

80.0 3863.10
80.5 3899.80
81.0 3936.84
81.5 3974.22
82.0 4011.96
82.5 4050.05
83.0 4088.52
83.5 4127.37
84.0 4166.61
84.5 4206.25

85.0 4246.30
85.5 4286.78
86.0 4327.69
36.5 4369.05
87.0 4410.87
87.5 4453.15
88.0 4495.93
88.5 4539.19
89.0 4582.97
89.5 4627.28
90.0 4672.12
90.5 4717.52
91.0 4763.49
91.5 4610.04
92.0 4857.20
92.5 4904.98
93.0 4953.40
93.5 5002.47
94.0 5052.23
94.5 5102.67

95.0 5153.83
95.5 5205.73
96.0 5258.39
96.5 5311.64
97.0 5366.09
97.5 5421.17
98.0 5477.10
98.5 5533.92
99.0 5591.65
99.5 5650.32
1

-------
 EPA    TEST    PROCEDURE
                                     Number
                            TP-204
                                              Page
                        of
 SUBJECT
 CHART RECORDER/MAINTENANCE
 Reference
 MANUFACTURER'S SERVICE MANUALS
                                             Data Form No.
                                             INSTR. LOGBOOK
 Responsible Organization
 INSTRUMENT SERVICES
 Test Witness/Review
 INSTRUMENT SERVICES LEADER/QUALITY ASSURANCE
 Type of Test Report
 CALIBRATION STICKER AND LOG BOOK ENTRY
 Report Distribution
 QUALITY ASSURANCE, INSTRUMENT SERVICES
                                             Computer Program
                                                              NONE
                                             Performance Interval
                                             MINIMUM;  90 DAYS ___
                                             Supersedes
                                             New	
                                             Superseded by
 REMARKS/COMMENTS
                            ORIGINAL KtLtAbt AKKKUVALb
 Office
   Section
Signature
Date
Program Mgmt
Quality Assurance
Lab Branch
Chief
Lab Branch
Support Services Chie.f_
                                    REVISIONS
Change
Letter
 Description of Change
        Approval
Date
                                     63

-------
REVISIONS:


CHART RECORDER CALIBRATION/MAINTENANCE
TEST PROCEDURE
PROCEDURE NO.
TP-204
pAftP 2 OF 3

1.0  PURPOSE

     To perform periodic recalibration and maintenance after periods of use
     or questionable performance.  Recalibration will assure accurate instrument
     output and prolong the useful life of the instrument.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Chart recorder, two channel model capable of measuring two variables
          on the same chart.  The recorder is a continuous balance potentiometer
          which responds to a d-c signal representing the value of the measured
          quantity.

     2.2  Typical chart recorders used may be:

               o    Honeywell 194 Electronik
               o    Varian G-14A-2
               o    Varian G-1110
               o    Hewlett-Packard 680
               o    Texas Instruments 4525-2, 7822-2  (4 pen)
               o    Texas Instruments 2596-2 (2 pen)

3.0  REFERENCES

     Each recorder listed in 2.2 has a manual showing theory/operation, maintenance
     and calibration procedures.  These manuals are available and should be
     reviewed by the instrument technicians.

4.0  REQUIRED EQUIPMENT

     The list of equipment in this section represents an example of the articles
     needed to perform a valid calibration.  It should be noted that manufacturers
     of specific equipment may list requirements for their own calibration items.

     4.1  Example of calibration equipment

               o    Calibrated precision voltage source.
                    Example: Honeywell Model 2746 portable potentiometer, 0-200
                    microvolt to 0-500 millivolt ranges.

               o    Test leads  (preferably with banana plugs)
               o    Calibration screwdrivers (1/8" and 1/4" bits)

5.0  PRECAUTIONS

     5.1  Calibration and adjustment of recorders should be accomplished by
          Instrument Service Technicians only.

     5.2  Safety precautions should be observed in using electrical equipment.
                                      65

-------
REVISIONS--

CHART RECORDER CALIBRATION/MAINTENANCE
TEST PROCEDURE
PROCEDURE NO.
TP-204
PAGP 3 OF__1_
 6.0  VISUAL INSPECTION

     6.1   Inspect slidewires for signs of wear.

     6.2   Inspect RECORDER for disconnected leads and/or broken wires.

 7.0  TEST ARTICLE PREPARATION

     7.1   Set  up calibration equipment as specified in applicable  service manual.

 8.0  TEST PROCEDURE

     Each manufacturer of chart recorders outlines specific calibration procedures
     common to their product.  Therefore, the test procedures for  chart recorder
     calibration should be taken from the manufacturer's text.  It is also
     suggested that routine maintenance should be accomplished prior to the
     calibration of each recorder.

 9.0  DATA INPUT

     9.1   The  date of calibration, type of instrument, serial number, and work
           performed is recorded in instrument calibration log book (see
           attachment).

 10.0 DATA ANALYSIS

     10.1 Observed readings and calibration input should be compared.

 11.0 DATA OUTPUT

     11.1  Calibration sticker showing the date of calibration and  the date the
           next  calibration is due is attached to the recorder.  Calibration
           data  sheet shall be filed in the instrument file and logged in the
           record book.

12.0 ACCEPTANCE CRITERIA

     12.1 Recorder must function within ±1 percent accuracy and repeatability
          following calibration.

13.0 QUALITY PROVISIONS

     13.1 Check to assure calibration has been completed at proper time intervals.

     13.2 Assure that calibration sticker has been placed on recorder.
                                      66

-------
            TP-204 ATTACHMENT No. 1
INSTRUMENT SERVICES  LOG  BOOK
                                     TEC//.
940757
                   &-Z9-

                   10 -11-7
H-Z9-74

I-I/-7S
L\ I-
 .. A
                    12-7-14

                    :z -9 " 74
                     P?/Ci> JO

-------
EPA TEST
PROCEDURE Nur
*er ""OS P.O. 1 Of «
SUBJECT
TEMPERATURE RECORDER CALIBRATION/MAINTENANCE
Reference
MANUFACTURER'S SERVICE MANUAL
Responsible Organization
INSTRUMENT SERVICES
Data Form No.
LOG BOOK
Computer Program
NONE
Test Witness /Review Performance Interval
INSTRUMENT SERVICES LEADER, QUALITY ASSURANCE MINIMUM: 90 DAYS
Type of Test Report
LOG BOOK ENTRY AND CALIBRATION STICKER
Report Distribution
QUALITY ASSURANCE, INSTRUMENT SERVICES
Supersedes
NEW
Superseded by
REMARKS/ COMMENTS
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Branch
Lab Branch


Section
Quality Assurance
Chief
Support Services Chief


Signature





Date





REVISIONS
Change
Letter
Description of Change
Approval

Date

69

-------
REVISIONS:
                    TEMPERATURE RECORDER CALIBRATION/MAINTENANCE

                           TEST    PROCEDURE
PROCEDURE  NO.
   TP-205	

PAGEi__OF _i__
1.0  PURPOSE

     To perform periodic re-calibration and maintenance after periods  of use
     and/or questionable performance.  Re-calibration of temperature
     recorders will assure accurate instrument output and prolong the
     instrument's useful life.

2.0  TEST ARTICLE DESCRIPTION

     Temperature recorders vary  in make, however, the operating principles
     are generally the same.   A  temperature probe (normally iron-constantan
     thermocouple) senses the  temperature and produces an unknown voltage
     which is in turn subtracted from a known voltage.  The difference
     in voltages is amplified  and displayed by the recorder

     2.1  Temperature recorders  vary in application, ranging from one
          channel to as many as  24 channels for measuring independent
          variables.

          The following recorders are representative of the types used
          in emission monitoring.

          o    Esterline Corp.,  24-channel, Model E1124E
          o    Honeywell, 24-channel, Model Elect. 19
          o    Honeywell, multi-channel, Model Elect 15
          o    Rustrax, single-channel, Model 2133

3.0  REFERENCES
     Each recorder listed in 2.1 has  a manual showing theory/operation,
     maintenance and calibration procedures.  Manuals of this nature
     must be made available to the  instrument technicians.

4.0  REQUIRED EQUIPMENT

     The list of equipment in this  section represents an example of
     the articles needed to perform a valid calibration.  It should
     be noted that manufacturers of specific equipment may list require-
     ments for their own calibration  items.
                                       71

-------
REVISIONS'
                    TEMPERATURE RECORDER CALIBRATION/MAINTENANCE

                           TEST    PROCEDURE
PROCEDURE  NO.
   TP-2Q5	
PAGE.
.OF
     4.1  Example of calibration equipment

          o    Precision voltage source  (used for input voltages
               from temperature-EMF equivalents) reference 0° C
               or 32° F.

          o    Thermocouple  extension wire

          o    Ice bath for  0° C or 32° F reference.

          o    Reference standard, Hewlett-Packard temperature indicator -
               Quartz digital

5.0  PRECAUTIONS

     5.1  Dangerous stray voltages exist.  Before touching connections,
          turn off power and check each terminal with a multimeter.

     5.2  Calibration and adjustment of recorders should be accomplished
          by Instrument Service technicians only.

6.0  VISUAL INSPECTION

     6.1  Inspect for obvious signs of wear.

     6.2  Inspect for disconnected leads and/or broken wires.

7.0  TEST ARTICLE PREPARATION

     7.1  Set up calibration equipment as specified in applicable
          service manual.

8.0  TEST PROCEDURE

     Each manufacturer of temperature recorders outlines specific
     calibration procedures  common to their product.  Therefore, the
     test procedures for the recorder calibration should be taken from
     the manufacturer's text.  It is also suggested that routine
     maintenance should be accomplished prior to the calibration
     of each recorder.

9.0  DATA INPUT

     9.1  The date of calibration, type of instrument, serial number,
          and work performed is recorded in instrument calibration
          log book (see attachment).
                                        72

-------
REVISIONS:

TEMPERATURE RECORDER CALIBRATION/MAINTENANCE
TEST
PROCEDURE
PROCEDURE NO.
TP-205
PAGF 4 OF 4
10.0 DATA ANALYSIS

     10.1 Compare observed temperature readings with the reference standard.

11.0 DATA OUTPUT

     11.1 Calibration sticker showing the date of calibration and the
          date the next due calibration is attached to the recorder.

     11.2 Information regarding the results of the calibration shall be
          filed with the instrument records.

12.0 ACCEPTANCE CRITERIA

     12.1 Temperature recorder must indicate ambient temperature within
          ±2 degrees of the true value.

     12.2 Temperature indicated must be within 1 percent of full scale at
          all points.

13.0 QUALITY PROVISIONS

     13.1 If acceptance criteria are not met, repair instrument and/or
          repeat calibration.
                                       73

-------
            TP-205 ATTACHMENT No. 1
  INSTRUMENT SERVICES  LOG BOOK

                     -29-
940757
(94
                   io-n-74
           l-li-75
12-7-74
A. A
TO

-------
EPA TEST
PROCEDURE Nur
Pa9e * of *
SUBJECT
BAROMETRIC PRESSURE
CALIBRATION AND CORRELATION
Reference Federal Register, Vol. 39, No. 101, May 23, 1974, Data Form No .
85.075-22 (jl T.™ n™i.
Responsible Organization
Chemical Analysis
Test Witness/Review
Correlation and Maintenance
Type of Test Report
Log Book Entry
Report Distribution chemistry Section,
Compliter Program
None
Performance Interval
Monthly
Supersedes
New
support services Superseded by i
REMARKS/ COMMENTS
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt.
Lab. Branch
Lab . Branch


Section
Quality Assurance
Chief
Support Services Chief


Signature





Date





111 RL-ViblONb
Change
Letter
Description of Change
Approval

Date

75

-------
REVISIONS:


BAROMETRIC PRESSURE
CALIBRATION & CORRELATION
TEST PROCEDURE
PROCEDURE NO.
TP-206
PAOF 2 OF 9

1.0  PURPOSE

     To calibrate the aneroid barometers used in the test call against a Fortin
     type barometer to assure accurate and uniform test cell readings.

2.0  TEST ARTICLE DESCRIPTION

     Aneroid barometer compensated for temperature, brass, scale 25.1-31.1
     inches of mercury (Hg), 0.02 subdivisions.

3.0  REFERENCES

     3.1  PRINCO Barometer  Instruction Booklet

     3.2  W.G. Brombacher,  D.P. Johnson, and J.L. Cross.,
          "Mercury Barometers and Manometers"
          NBS Monograph 8,  May 1960.

4.0  REQUIRED EQUIPMENT AND CONDITIONS

     4.1  Fortin type barometer, 1/4 inch bore, reading by vernier to
          0.01 in. Hg

     4.2  Rack for hanging  the aneroid barometers

     4.3  Temperature controlled room of +J3QF.

5.0  PRECAUTIONS

     5.1  The Fortin type barometer readings are corrected for temperature
          and gravity.  The aneroid barometer is set to the corrected baro-
          meter reading.

     5.2  The aneroid barometers may indicate a slightly different reading from
          one cell to another due to variations in the air handling system.
          Large variations  indicate a need for calibration or replacement.

     5.3  Important factors which could affect the reading of the height
          of the mercury are

          o    Lighting - Proper illumination is essential to define the loca-
               tion of the  crown of the meniscus.  Precision meniscus sighting
               under optimum viewing conditions can approach +_ 0.001 in.
               Contact between index and mercury surface in the cistern, judged
               to be made when a small dimple in the mercury first disappears
               during adjustment, can be detected with proper lighting to much
               better than  +_ 0.001 in.

          o    Temperature  - To keep the uncertainty in height within 0.01%
               (0.003 in. Hg), the mercury temperature must known within
                                        77

-------
REVISIONS:

BAROMETRIC PRESSURE
CALIBRATION & CORRELATION
TEST PROCEDURE
PROCEDURE NO.
TP-206
PAGF 3 OF 9
     5.4
      ±1  F.  Although  it is  generally  assumed  that the  scale and mercury
      temperatures  are identical,  the  scale  temperature need not be
      known  to better  than ±10 F for comparable  accuracy-   Uncer-
      tainties caused  by nonequilibrium  conditions could be avoided by
      installing  the barometer in  a uniform  temperature room.

 o     Alignment - Vertical alignment of  the  barometer tube  is  required
      for an accurate  pressure determination.  The Fortin barometer,
      designed to hang from  a hook, does not of  itself  hang vertically.
      This must be  accomplished by a separately  supported ring encir-
      cling  the cistern;  adjustment screws control the  horizontal
      position.

 o     Readings -  The most reliable readings  are  obtained when  the tem-
      perature has  not changed greatly over  the  past four hours.   When
      reading the barometer  the reader's eye should be  in the  same
      horizontal  plane as the top  of the mercury meniscus and  the lower
      edge of the vernier plate.   This position  can be  checked by getting
      the  eye in  line  with the bottom of the vernier plate  and the bottom
      of  the metal  guide  in  back of the mercury  column  directly in back
      of  the vernier plate.

      Readjustment  to  zero should be made whenever necessary in reading
      the  barometer; i.e., the adjusting screw at  the bottom of the
      reservoir casing  should be manipulated until the  surface of the
      mercury exactly  coincides with the tip of  the ivory zero point
      which  is visible  inside the reservoir.

      The  height  of the meniscus will be greater on a rising barometer
      than on a falling barometer.   In order to bring the meniscus to
      its  approximate  average height,  tap the barometer  lightly with
      your fingers before taking a reading.

If it is  desired to convert an english reading  to a metric reading,
or vice versa, always apply the temperature and gravity corrections
before making conversion.
6.0  VISUAL INSPECTION
     6.1
     6.2
If an aneroid barometer has a cracked glass or dented case the complete
barometer should be replaced.   Do not attempt to recalibrate as the
internal movements may have been also damaged.

If the mercury appears dull or tarnished, it is an indication that
the mercury has become contaminated in some way.  It frequently occurs
when air, dirt, and moisture are admitted into the barometer tube.
In such event the instrument will no longer give accurate readings.
For proper cleaning the instrument should be returned to the factory.

-------
REVISIONS:
    BAROMETRIC PRESSURE
CALIBRATION & CORRELATION

   TEST    PROCEDURE
PROCEDURE NO.
       TP -206

PAGE JL-OF JL_
 7.0   TEST ARTICLE PREPARATION

                                                                            o
       7.1   The aneroid barometers to be calibrated should be hung in the ±3 F
            temperature controlled room for a minimum of 4 hours to allow them
            to come to equilibrium with the ambient conditions.
                                 A Fortin-type bnromctcr.
                                             Closed end
                                           vacuum-referred
                                              Reading level
                                              Glass tube
                       Glass cylinder
                      ambient-vented'
                         cistern
                          Ivory index
                           point
                                              (— Leather bag
                                              Dotum-adjustinrj
                                                 screw
                                       79

-------
REVISIONS:
           BAROMETRIC PRESSURE
        CALIBRATION & CORRELATION

           TEST    PROCEDURE
PROCEDURE  NO.
    TP-206	

PAGE.JLOF _JL.
 8.0  TEST PROCEDURE

      The test requires three basic  procedures:  A. Reading the mercury baro-
      meter, B. Calibration of the aneroid barometer and C.  Correlation of
      the test cell barometers.
 Test Sequences
      101A
               Test Description

In reading a barometer of the  Fortin type,
which is the usual laboratory  precision type,
first obtain the temperature of  the case
from the small thermometer attached midway
between the top and bottom of  the
instrument.  Then adjust the
mercury in the reservoir to the
fixed point (an ivory pin), so that
the tip of the pin and its image
upon the mercury surface coincide.
Tap the barometer case gently  to be
sure that the mercury is not stuck
in the tube and verify the zero
setting.  Now bring the vernier
down until the white background
is cut off at the highest point  of
the meniscus.   The reading is  the
uncorrected barometric height.
     Data  Output
                                                                      Pressure,
                                                                      un-corrected
      102A      The standard temperature  for the
                English scales  is  62 F.;  the
                standard temperature for  the Metric
                scales is 0 C.   The standard temp-
                erature for the density of mercury
                is 0 C. or 32 F.   Since the scales
                and the mercury have different co-
                efficients or expansion,  the pressure
                indications will be affected by
                variations in temperature; there-
                fore ,  in order  to  obtain  the
                true pressure every reading
                must be corrected  for tempera-
                ture.   The Temperature Cor-
                rection Tables  combines the
                corrections for length of
                the scales and  the density of
                mercury.

                Further,  the pressure indication will
                be affected by  the gravity of the
                place at which  the reading is taken.
                Latitudes from  0  to 45   have a
                subtractive correction; latitudes
                       o     o
                from 46  to 90   have an additive
                correction.  More  precise
                                                      Temperature
                                                      correction
                                                      factor
                                                      Gravity
                                                      correction
                                                      factor
                                       80

-------
REVISIONS:
   BAROMETRIC PRESSURE
CALIBRATION & CORRELATION

  TEST    PROCEDURE
PROCEDURE  NO.
   TP-206	

PAGEJL-OFJL_
 Test Sequence                 Test Description                        Data  Output


                determinations of the  true pressure may be
                made by using the Gravity Correction Tables
                in conjunction with the  observed readings
                corrected for temperature.

                EXAMPLE;  Assume the barometer reads 29.91"
                at a temperature of 75°F.  Table 1 gives the
                temperature correction for every two degrees
                Fahrenheit and every one inch of atmospheric
                pressure.  Interpolating, we find the
                correction to be -.125".  The reading cor-
                rected for temperature,  therefore, is 29.91"
                -.125', or 29.785". If  the reading is
                being taken at a latitude of 42° the
                correction for gravity given in Table 2 is
                -.010" which makes the true pressure 29.785"
                -.010, or 29.775" which, if working to one
                hundredths of an inch, could be rounded off
                to 29.78".

      101B      After the aneroid barometers have attained            Calib. Date
                equilibrium read the Fortin barometer and             Log Book
                adjust the aneroid barometers at the                  Entry
                corrected reading using  the adjusting
                screw on the back of the barometer.  Gently
                tap each gauge before  taking the reading.
                Cover the adjusting screw with a piece of
                tape to discourage tampering.

      101C      Correlation is accomplished by reading all            Log Book
                the test cell barometers in their usual               Entry  By
                position once a week.                                 I.D. Number
                                       81

-------
REVISIONS:


BAROMETRIC PRESSURE
CALIBRATION & CORRELATION
TEST PROCEDURE

PROCEDURE NO.
TP-206
PAGE
7 OP 9

TEMPERATURE CORRECTION TABLE — Table 1 — English System
To reduce the reading of the barometer to standard temperature
i Tempera-
ture in
Degrees F.
60°
62
64
66
.68
70
72
74
76
78
80
82
84
06
88
90
92
94
96
98
100
Observed Reading of the Barometer
20"
21" 22" 23" 24"
25" | 26" | 27"
in Inches
28" 29

n
\
30" | 31"
ALL CORRECTIONS SUBTRACTIVE
0.057
.060
.064
.068
.071
.075
.078
.082
.086
.089
.093
.096
.100
.104
.107
.111
.114
.118
.122
.125
.129
0.060
.063
.067
.071
.075
.079
.082
.086
.090
.094
.097
.101
.105
.109
.113
.116
.120
.124
.128
.131
.135
0.062
.066
.070
.074
.078
.082
.086
.090
.094
.098
.102
.106
.110
.114
.118
.122
.126
.130
.134
J138
.142
0.065
.069
.074
.078
.082
.086
.090
.094
.098
.103
.107
.111
.115
.119
.123
.127
.132
.136
.140
.144
.148
0.068
.073
.077
.081
.085
JD90
.094
.098
.103
.107
.111
.116
.120
.124
.129
.133
.137
.142
.146
.150
.154
0.071
.076
.080
.085
.089
.094
.098
.103
.107
.112
.116
.121
.125
.130
.134
.138
.143
.147
.152
.156
.161
0.074
.079
.083
.088
.093
.097
.102
.107
.111
.116
.121
.125
.130
.135
.139
.144
.149
.153
.158
.163
.167
0.077
.082
.086
.091
.096
.101
.106
.111
.116
.120
.125
.130
.135
.140
.145
.150
.154
.159
.164
.169
.174
0.080
.085
.090
.095
.100
.105
.110
.115
.120
.125
.130
.135
.140
.145
.150
.155
.160
.165
.170
.175
.180
0.082
.088
.093
.098
.103
.109
.114
.119
.124
.129
.135
.140
.145
.150
.155
.161
.166
.171
.176
.181
.187
0.085
.091
.096
.101
.107
.112
.118
.123
.128
.134
.139
.145
.150
.155
.161
.166
.172
.177
.182
.183
.193
0.088
.094
.099
.105
.110
.116
.122
.127
.133
.138
.144
.149
.155
.161
.166
.172
.177
.183
.188
.194
.200
82

-------
REVISIONS:




BAROMETRIC PRESSURE
CALIBRATION & CORRELATION
TEST PROCEDURE


PROCEDURE NO.
TP-206
PAGE_a_OF J2 —
GRAVITY CORRECTION TABLE — Table 2 — English System
To reduce the reading of the barometer to standard gravity
Lati-
tude
o«
5
10
15
20
25
30
32
' 34
36
36
40
42
44
46
48
50
55
60
65
70
75
80
85
90
Observed Reading of the Barometer in Inches
20" 21" 22" 23" 24" 25" 26" | 27" 28"
29" | 30"
LATITUDE On TO 45° THE CORRECTION IS TO BE SUBTRACTED
LATITUDE 46° TO 90° THE CORRECTION IS TO BE ADDED
-0.054
.053
.050
.047
.041
.035
.027
.024
.021
.017
.014
.010
.006
-0.003
+0.001
.005
.008
.017
.026
.033
.040
.045
.049
.051
+0.052
-0.056












.055
.053
.049
.043
.037
.029
.025
.022
.018
.014
.011
.007
-0.003
+0.001









.005
.009
.018
.027
.035
.042
0.47
.051
.054
+0.055
-0.059
.058
.055
.051
.045
.038
.030
.026
-023
.019
.015
.011
;oo7
-0.003
+0.001
.005
.009
.019
.028
.036
.044
.049
.054
.056
+0.057
-0.062
.061
.058
.053
.047
.040
i031
.028
.024
.020
.016
.012
.007
-0.003
+0.001
.005
.010
.020
.029
.038
.046
.052
.056
.059
+0.060
-0.064
.063
.060
.056
.050
.042
.033
.029
.025
.021
.016
.012
.008
-0.003
+0.001
.006
.010
.021
.031
.040
.048
.054
.059
.061
+0.062
-0.067
.066
.063 ;
.058
.052
.043
.034
.030
.026
.022
.017
.013
.008
-0.003
+0.001
.006
.010
.021
.032
.041
.050
.056
.061
.064
+0.065
-0.070
.069
.066
.060
.054
.045
.035
.031
.027
.022
.018
.013
.008
-0.004
fO.OOl
.006
.011
.022
.033
.043
.052
.058
.063
.067
J-0.068
-0.072
.071
.068
.063
.056
.047
.037
.032
.028
.023
.018
.014
.009
-0.004
»-0.001
.006
.011
.023
.034
.045
.053
.061
.066
.069
* 0.070
-0.075
.074
.071
.065
.058
.049
.038
.034
.029
.024
.019
.014
.009
-0.004
+0.001
.006
.012
.024
.036
.046
.055
.063
.068
.072
+0.073
-0.078
.077
.073
.067
.060
.050
.040
.035
.030
.025
.020
.015
.009
-0.004
40.001
.007
.012
.025
.037
.048
.057
.065
.071
.074
10.075
-0.080
.079
.076
.070
.062
.052
.041
.036
.031
.026
.020
.015
.010
-O.Q04
+ 0.001
.007
.012
.026
.038
.050
.059
.067
.073
.077
-1 0.078
83

-------
REVISIONS:

BAROMETRIC PRESSURE
CALIBRATION & CORRELATION
TEST PROCEDURE
PROCEDURE NO.
TP-206
PAGE 9 OF _2_—
9.0  DATA INPUT

     9.1  Enter calibration dates in log book by l.D. number.  Indicate ad-
          justed or not adjusted.

     9.2  Enter the amount of deviation from true barometric pressure in the
          instrument log book.

10.0 DATA ANALYSIS
     None required

11.0 DATA OUTPUT

     11.1 A handwritten copy of the correlation data goes to Quality Assur-
          ance management.

12.0 ACCEPTANCE CRITERIA

     12.1 In order to achieve 0.1% accuracy the barometer readings should cor-
          relate among themselves within +_ 0.03 in.  Hg.

     12.2 Correlation should be established over 28.5 to 30.0 in. Hg. range.

13.0 QUALITY PROVISIONS

     13.1 At the Factory the Fortin-Type Barometers  are  adjusted as nearly as
          possible to a zero correction by comparison with a certified stan-
          dard.   The adjustment is so made that no further correction for capil-
          larity need be made.

-------
300

-------
 Section 300
VERIFICATION

-------
EPA TEST
PROCEDURE Nur
^^ T*-301 Paae 1 of 8
SUBJECT
CVS SYSTEM VERIFICATION BY TRACER GAS INJECTION
Reference FEDERAL REGISTER, VOL. 138,
June 28 , 1973 -
Aooendix III
Responsible Organization
CORRELATION/MAINTENANCE
Test Witness /Review
QUALITY ASSURANCE
Type of Test Report
COMPUTER PRINT-OUT
NO. 124, Data Form No.
301-01
Computer Program
SAQF: CALIBCK
Performance Interval
SEE WEEKLY/SEC 13.0
Supersedes
NEW
Report Distribution Superseded by
QUALITY ASSURANCE/TEST OPERATIONS/CORRELATION & MAINTENANCE
REMARKS/ COMMENTS
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Branch
Lab Branch
Lab Branch

Section
Quality Assurance
Chief
Test Operations Chief
Support Services Chief

Signature





Date





REVISIONS
Change
Letter
Description of Change
Approval

Date

87

-------
REVISIONS:


CVS SYSTEM VERIFICATION
TEST
PROCEDURE
PROCEDURE NO.
TP-301
PAGE_2-OF J —
1.0  PURPOSE

     To verify that the CVS sampling system, its associated analyzers, and
     subsequent data analysis will determine the correct mass value of a
     quantity of gas injected into the system.  The actual or theoretical mass
     value is compared to the indicated mass value to obtain the accuracy (% error)
     of the system.

2.0  TEST ARTICLE DESCRIPTION

     2.1  A constant volume sample which meets the requirements stated in
          Federal Register 85.075-20 (see procedure # 201 for calibration
          procedure).

     2.2  A gas analysis system meeting requirements in Federal Register 85.075-20.

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 124, Appendix III and 85.075-20.

     3.2  EPA, Ann Arbor, Preventive Maintenance Guideline, Section V.

4.0  REQUIRED EQUIPMENT

     4.1  Equipment required for "Bomb Method"

          4.1.1     Supply cylinder of pure tracer gas.  Normally propane is used,
                    however carbon monoxide  (CO) may be used as an alternative.

          4.1.2     Small laboratory cylinder filled with pure tracer gas from the
                    supply cylinder.  The "bombs" normally have a volume of
                    16,000 cubic centimeters.

          4.1.3     Injection fitting.

          4.1.4     Analytical balance for weighing cylinder  (see procedure # 101,
                    sec. 7.2, for calibration procedure).

     4.2  Equipment required for Critical Flow Orifice  (CFO) method.

          4.2.1     Supply cylinder of 99.5% pure tracer gas

          4.2.2     CFO kit.

          4.2.3     Injection fitting.

          4.2.4     Thermometer.

-------
REVISIONS:

CVS SYSTEM VERIFICATION
TEST
PROCEDURE
PROCEDURE NO.
TP-301
DAftF 3 OF _A_
5.0  PRECAUTIONS
     5.1  Carbon monoxide is an odorless,  extremely poisonous gas.  Therefore, when
          it is used as a tracer gas,  the safety precautions outlined below must
          be observed.

          1.   Two operators experienced in pressurized gas handling should be in
               attendance.

          2.   Provide adequate ventilation in the work area.  Turn on the dyna-
               mometer test cooling fan.

          3.   Before connecting the CFO kit to the CO bottle, prepare the SAF-
               CO-Meter bulb for use as specified in the instructions provided.
               Check storage date on the glass ampoules.

          4.   After connecting the CO bottle, with the CVS running and the CFO
               outlet line inserted into the exhaust plenum, open the CO bottle
               valve just enough to show full bottle pressure on the regulator
               high pressure gauge.  Starting at the bottle valve, check for leaks
               at all fittings using soap solution and/or the SAF-CO-Meter.  If
               a leak is discovered, close the CO bottle valve first before
               retightening or servicing.

          5.   Use the SAF-CO-Meter to monitor ambient air during the test.

          6.   Shut off the CO bottle valve before stopping the CVS.

6.0  VISUAL INSPECTION

     6.1  Inspect the equipment set-up to insure the system is leak-tight.

7.0  TEST ARTICLE PREPARATION

     7.1  Preparation for "Bomb" injection.

          7.1.1     Fill the evacuated bomb cylinder with tracer gas from the
                    supply cylinder.  The  regulator (output) should be set at
                    40 PSIG for propane (blue cylinder)  and 80 PSIG for carbon
                    monoxide (gray cylinder).  Transfer the gas for three minutes.

          7.1.2     Run the CVS for five minutes and allow the pump inlet tempera-
                    ture to stabilize  at 100°F.   Attach the injection fitting
                    and the auxiliary  temperature sensor to the spare fitting on
                    the pump elbow.

          7.1.3     Zero the CVS counters,  timer and evacuate the sample/background
                    bags.   Replace sample  filter and assure the filter holder is
                    completely closed.   Set  the  flow rates at 5.0 cfh.
                                     90

-------
REVISIONS:
                              CVS SYSTEM VERIFICATION
                          TEST    PROCEDURE
PROCEDURE NO.
     TP-301
PAGE_1_OF
                                                                            8
       7.2  Preparation for CFO method.

           7.2.1     Connect the injection fitting to the dilution box so  that the
                     gas is injected into the dilution air stream.

           7.2.2     Couple the injection fitting to the CFO apparatus.

           7.2.3     Attach the thermometer in the area of the CFO temperature
                     stabilizing coil.

           7.2.4     Lock the Hiese gauge in vertical position on the CFO  and set
                     the pointer to zero.

           7.2.5     Run the CVS for 3 minutes and allow the flow rate and
                     temperature to stabilize.
                                                            Flexible Hose
                              CFO  INJECTION SET-UP
           7.2.6     Follow steps in 7.1.3.

           7.2.7     Connect the CFO to the gas supply cylinder (CO or propane),
                     open the valves and adjust the  regulator to approximately
                     70 psig for propane and 50 psig for carbon monoxide.
                                      91

-------
REVISIONS:
                              CVS SYSTEM VERIFICATION
                           TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                       TP-301
                                                 PAGEj_OF
                                                                               8
  8.0  TEST PROCEDURES

      Two methods of CVS system verification are presently in use.  Section I
      describes the steps for the Bomb method and Section II outlines the CFO
      technique.
  Test Sequence

       101
             SECTION I "THE BOMB"

                   Test Description

Weigh the bomb and record initial weight on data
sheet.
       102       Sample the dilute mixture in the normal manner
                 (procedure #707).

       103       Connect the bomb to the  injection probe and open
                the bomb valve.   Regulate the flow rate to
                2.0 ±.25 cfh for propane or 12.0 ±.25 cfh for CO.

       104       While gas is being sampled, check and record the
                following:

                     o    Pump inlet pressure.

                     o    Pump outlet pressure.

                     o    Barometric pressure.

                     o    Ambient room temperature.

                     o    CVS pump inlet temperature.

       105       After the tracer gas has been sampled for 15 minutes,
                close the bomb valve, purge the injection fitting
                with nitrogen and disconnect from the injection
                fitting.

       106       Stop sampling the dilute mixture.  Record the pump
                revolutions and sample time.

       107       Analyze the sample and background bags.  Record
                their concentrations on  the data sheet.

       108       Have the bomb reweighed  and record final weight to
                the nearest milligram.
Data Output

gms
                                                     P.   "fluid
                                                       in

                                                     P ^  "fluid
                                                       out
                                                         "Hg
                                                     Twb/Tdb  F
                                                      T.
                                                       in
                                                      Revs
                                                      t,  sees.
                                                            ppm
Cone ,  ppm
Cone ,
    s
                                                      gms

-------
REVISIONS:
                               CVS SYSTEM VERIFICATION
                           TEST    PROCEDURE
                                                PROCEDURE NO.
                                                      TP-301
                                                PAGE.JLOF
                                                                              8
  Test Sequence
       201
       202
       203
       204


       205

       206
           SECTION II CFO TECHNIQUE

               Test Description

When CFO pressure gauge has stabilized,  begin  sampling
the dilute mixture and background air.

Monitor and record the CFO temperature  and pressure
several times during the sample period.
NOTE:  If the pressures and temperatures have  not
varied more than 0.3 psi and 0.5 F, record the
average.  If the variation is greater perform  an
additional CFO injection.

While the gas is being sampled, check and record the
following:

     o    Pump inlet pressure

     o    Pump outlet pressure

     o    Barometric pressure

     o    Ambient room temperature

     o    CVS pump inlet temperature

After 10 minutes, stop the sampling mode.  Record
the revolutions and sample time.

Shut off the CFO gas supply cylinder.

Analyze the sample and background bags.   Record the
concentration values on the data sheet.
Data Output
T  °F
                                                                      P.   "fluid
                                                                       in

                                                                      P    "fluid
                                                                       out
                                                                          "Hg
                                                                      Twb/Tdb  F

                                                                      T.    °F
                                                                       in
revs
t, sees.
Cone ,  ppm
Cone ,  ppm
    s
                                      93

-------
REVISIONS:

CVS SYSTEM VERIFICATION
TEST PROCFniJPF
PROCEDURE NO.
TP-301
PAGF_7 OF 8
9.0  DATA INPUT

     9.1  Check and assure all data has been properly entered on data sheet 301-01.

     9.2  Submit data to Data Branch for computer analysis (SAQF:  CALIBCK).

10.0 DATA ANALYSIS

     10.1 Analysis of the "bomb" method is accomplished by the SAQF: CALIBCK
          computer program.  This program compares the indicated mass of the
          tracer gas versus the actual mass determined by gravimetric difference.

     10.2 Analysis of the CFO technique is also performed by the SAQF: CALIBCK
          program.  The observed concentration is compared to the calculated
          concentration to determine the accuracy (% error)  of the system.

11.0 DATA OUTPUT

     11.1 A computer print-out indicating percent error of the system.

     11.2 The results are stored in a computer file for future reference.

12.0 ACCEPTANCE CRITERIA

     12.1 The acceptable error band for CVS system verification checks is
          ±2 percent.

13.0 QUALITY PROVISIONS

     13.1 The results of the tests should be kept on file with Quality Control
          and analyzed statistically to determine average error/variation.

     13.2 If the results of any test exceed the prescribed error band, corrective
          action should be initiated and the procedure repeated.

     13.3 If three consecutive tests are not within the error band, the CVS shall
          be removed from line operation and recalibrated.

     13.4 The Quality Assurance section should suggest possible cause of error by
          referencing the following troubleshooting guideline.

-------
REVISIONS:


CVS SYSTEM
VERIFICATION
TF^T PROCEDURE
1 h»W 1 1 I\^^X« k k* Wl\k
PROCEDURE NO.
TP-301
pAftF 8 OF 8

Positive Error (Indication is higher than true value)

     1.   Calculated V  is greater than actual V .
                      o    ^                    o

          a.   Original calibration in error.

     2.   Pump inlet temperature recorder is reading low.  A 6 F
          discrepancy over the test period will give a 1% error.

     3.   Pump inlet indicator is reading high.  A 3.5 in. HO high
          reading will give 1% error.

     4.   Background concentration reading is too low.  Check analyzer
          zero.  Check leakage at floor inlet.

     5.   Analyzer is reading high.  Check span.

     6.   Barometer reading is in error (too high).  Barometric pressure
          reading should be gravity and temperature corrected.

     7.   Revolution counter is reading high. (Check pump speed and
          counters.

     8.   Mixture is stratified causing the sample to be higher than
          the average concentration in the mixture.

Negative Error (Indication is lower than true value)

     1.   Calculated V  is less than actual V .
                      o                      o
          a.   Original calibration in error.

          b.   Pump clearances decreased due to influx of some surface
               adherent material.

     2.   Pump inlet temperature recorder is reading high.

     3.   Pump inlet pressure indicator is reading low.

     4.   Background concentration reading is too high.

     5.   Analyzer is reading low.

     6.   Barometer reading is in error (too low) .

     7.   Revolution counter is reading low.

     8.   There is a leak into the sampling system.  Pressure check the
          lines and fittings on the intake side of sample transfer pumps
          on both the CVS and analyzer console.
                            95

-------
                             CVS SYSTEM VERIFICATION BY TRACER
                              GAS_INJECTION - TEST DATA SHEET







PREVIOUS
CVS
TEST NO.




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CVS
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                    *NOTE:  Specify  the  column height,  units,  and
                            fluid specific  gravity shown on the
                            manometert
Form 301-01

-------
                                                        TP-301
                                                        Attachment No.  1
           CVS SYSTEM VERIFICATION BY  TRACER  GAS  INJECTION
PREV.CVS  CVS  ANALYZER  TEST
TEST NO.  UMIT  TRAIN    DATE
 0-   0   12C    19     3-31-75

COMMENTS: PROPANE  INJECTION
                                CVS         AMrilENT CONDITIONS
                               HOURS  UAROMI-TER  DRY HULH  Wf-.T
                               1196.5    28.96     72.8      58.1

                                RAAU
                               CVS PUMP
          PRESSURE
TEMP     IN    OUT
102.7  28.75   15.35

     MANOMETER SPECIFICATIONS:  IN OF   1.75  SPECIFIC GRAVITY FLUID
                                             RPM
                   COUNTS  SECONDS    RPM   RATIO    CFR      SCFM
                    8101.   333.2   1458.«  0.9994  0.28295  J26.89
        METER READING
 GAS   SAMPLE  BACKGND
 HC     8^.8      0.9
RANGE
 S B
 4 <*
                                ANALYZER
                                                         CALCULATED
                                 CONCENTRATION  (PPM)       MASS
                             SAMPLE  BACKGND  CORRECTED    (GRAMS)
                             254.40     2.70    251.70      8.023
                                 CFO
            ORIFICE PRESSURE
GAS   TEMP   PSIG     PSIA
HC    74.5   73.40   87.63
                                      SCFM
                                    .0275395
                    CONCENTRATION
                        (PPM)
                       252.74
% ERROR
  -0.412
                                    97

-------
EPA TEST
PROCEDURE NU'
Tiber
TP-302 Page i of 6
SUBJECT
DYNAMOMETER CALIBRATION VERIFICATION
Reference
EPA, ANN ARBQR,
MATNTRNANPF. MAMTIAT.
Responsible Organization
CORRELATION/MAINTENANCE
Data Form No.
•3D9-.ni
Computer Program
DYNOCK:SAQE
Test Witness /REVIEW Performance Interval
CORR. AND MAINT. LEADER, QUALITY ASSURANCE WEEKLY
Type of Test Report
COMPUTER PRINT-OUT
Supersedes
NEW
Report Distribution Superseded by
QUALITY ASSURANCE/TEST OPERATIONS/CORRELATION AND MAINT.
REMARKS/ COMMENTS !
ORIGINAL RELEASE APPROVALS
Office
PROGRAM MGMT
LAB. BRANCH
LAB. BRANCH


Section
QUALITY ASSURANCE
TEST OPERATIONS CHIEF
SUPP. SERVICES CHIEF


Signature





Date





REVISIONS !
Change
Letter
Description of Change
Approval

Date
i
i
i
99

-------
REVISIONS:
                      DYNAMOMETER CALIBRATION VERIFICATION

                           TEST    PROCEDURE
PROCEDURE  NO.
   TP-302	

PAGE_2_QF  6
1.0  PURPOSE

     To verify the dynamometer calibration by a "short-cut method of periodic
     checks used for the determination of actual power absorption.

2.0  TEST ARTICLE DESCRIPTION

     2.1  A chassis dynamometer, having the capabilities described in the Federal
          Register, Part 85, Section 85.075-15.

     2.2  Associated speed and horsepower meters.

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 124, June 28, 1973,  85.075-15.

     3.2  EPA, Ann Arbor,  Preventive Maintenance Guidelines,  Section III.

     3.3  Clayton Manual for ECE-50 chassis dynamometer, p.  3-4.

4.0  REQUIRED EQUIPMENT

     4.1  Light weight test vehicle.

     4.2  Tachometer generator assembly.

     4.3  Strip chart recorder, Varian 614A.

     4.4  Stop watch or electronic timing device.

5.0  PRECAUTIONS

     5.1  Inflate tires to 45 psi to protect against overheating and wear.

     5.2  Align vehicle on dynamometer.

     5.3  Position vehicle cooling fan within 12 inches of vehicle radiator to
          prevent overheating.

     5.4  Insure vehicle exhaust is properly vented.

     5.5  Restrain vehicle with tie-down and safety chocks.

6.0  VISUAL INSPECTION

     6.1  Check equipment  set-up.

7.0  TEST ARTICLE PREPARATION

     7.1  Check the speed  and power meters for proper calibration.   (See
          procedure #202).
                                        101

-------
REVISIONS:
                       DYNAMOMETER CALIBRATION VEHIFICATION

                          TEST    PROCEDURE
PROCEDURE NO.
     TP-302

PAGE .2	OF *	
     7.2  Install tachometer generator on  the dynamometer frame.  Line up the
         tach generator pulley with the shaft adaptor pulley.  Insure that the
         center to center pulley distance is the same as the factory installed
         tach generator.

     7.3  Attach front roll tachometer generator electrical  leads to the Varian
         chart recorder.

     7.4  Place the vehicle on the dynamometer and attach the vehicle restraint
         system.   (Winch and cable).

     7.5  Disengage the roll brake.

     7.6  Adjust recorder zero.
                                     102

-------
REVISIONS:
                        DYNAMOMETER CALIBRATION VERIFICATION

                           TEST    PROCEDURE
PROCEDURE  NO.
    TP-302
PAGE.1-OF
 8.0  TEST PROCEDURES

      The following steps outline the short-cut coast down method for verifying
      the dynamometer calibration.

           TEST SEQUENCE             TEST DESCRIPTION               DATA OUTPUT

                101           Accelerate vehicle to 60 mph and
                              hold  steady.  Calibrate the chart
                              recorder at 60 mph full scale.

                102           Check the calibration of chart  at    55 =  	divs.
                              55, 50, and 45 mph.  Insure that     45 =  	divs.
                              the 55 and 45 mph points are easily
                              identified.

                103           Bring the vehicle to a complete stop.
                              Re-zero the recorder and set dyno
                              inertia to 4000 Ibs.

                104           Measure the recorder chart speed     Chart Speed
                              with  a stopwatch or other timing     (inches/mins)
                              mechanism.  This should be repeated
                              at least 3 times for an accurate mea-
                              surement of the distance the paper
                              travels in one (1) minute.
                              NOTE:     Alternate method of measuring
                                        elapsed time:  Direct measure-
                                        ment of time elapsed  between
                                        55 mph and 45 mph can be accom-
                                        plished by starting electronic
                                        timer at 55 mph and stopping
                                        at 45 mph.  This method will
                                        eliminate interpolation of
                                        chart method.

                105           Operate the vehicle at a steady 50 mph
                              and set Hp to indicated setting needed
                              for actual power absorption of  12.0 Hp.

                106*           Increase the vehicle speed to 60 mph
                              and use rear cable winch to pull vehicle
                              off the front drive roll.  Release
                              accelerator and allow vehicle to slow
                              down.
                                       103

-------
REVISIONS:
                      DYNAMOMETER CALIBRATION VERIFICATION
                          TEST    PROCEDURE
                                       PROCEDURE NO.
                                       PAGE-5-.OF
     TEST SEQUENCE

          107



          108
          109
              TEST DESCRIPTION

Measure  the time for the  roll to
slow from 55 MPH to 45 mph.  Record
time.

Bring vehicle speed as indicated
on speed meter to within  ±5 mph
of the front roll speed and
slowly loosen winch to allow the
drive tires to contact the front
roll.

Repeat steps 106-108 two  addi-
tional times and record.
DATA OUTPUT
 t, sees.
                                                                  t, sees.
                                     104

-------
REVISIONS:

DYNAMOMETER CALIBRATION VERIFICATION
TEST PROCEDURE
PROCEDURE NO.
TP-302
PAOF 6 OF_!_
9.0  DATA INPUT

     9.1  Complete data form 302-01 and submit it for analysis.

10.0 DATA ANALYSIS

     10.1 Analyze the data using the DYNOCKrSAQE program.

11.0 DATA OUTPUT

     11.1 Data sheet showing roll down times, signed by responsible technician.

12.0 ACCEPTANCE LIMITS

     12.1 The average time for coastdowns should be within 1 second,  (calculated)

13.0 QUALITY PROVISIONS

     13.1 If coastdown times are outside of the prescribed limits corrective
          action and a complete re-calibration will be instituted.
                                       105

-------
                                    COASTDOWN CHECK FOR CLAYTON DYNO
    DATE
                                         DYNO
      INHUTIA
      WEIGHT
110 RSI-POWER
  ' SET
ACT. COASTDOWN TIME
       IN SEC.
CALC. COASTDOWN TIME
        IN SEC.
DIFFERENCE
  IN SEC.
      2000
                                                   14.63
      3000
                                                   17.68
g
      4000
                                                   20.24
      5000
                                                   22.66
      5500
                                                   24.02
   FORM 302-01
                                         Signature

-------
  EPA    TEST   PROCEDURE
                                      Number
                            TP-303
                                                                Page
                                                        of
  SUBJECT
   NO  Efficiency Check
  Reference  Federal Register, Vol. 39, No. 101,
   May 23. 1974 - Sec; 85.075-23	
                                             Data Form No.
                                              303-01
  Responsible Organization
   Correlation/Maintenance
                                             Computer Program
                                              NOXCK:SAQE
  Test Witness/Review
   Corr. and Maint. Leader, Quality Assurance
  Type of Test Report
   Computer Print-out
  Report Distribution
Quality Assurance, Test Operations, Correlation and Maint.
                                             Performance Interval
                                             Weekly; Monthly
                                             Supersedes
                                             New	
                                             Superseded by
  REMARKS/COMMENTS
                             ORIGINAL RELLA5E APPROVALS
  Office
Program Mgmt
Lab. Branch
Lab.Branch
     BrancTT
   Section
Quality Assurance
Chief
Test Operations Chief
Supp. Services Chief
Signature
Date
                                     REVISIONS
 Change
 Letter
 Description of Change
        Approval
Date
                                      107

-------
REVISIONS:

NO EFFICIENCY CHECK
x
TEST
PROCEDURE
PROCEDURE NO.
TP-303
PAOF 2 OF ,5
 1.0 PURPOSE

     To determine the conversion efficiency of the NO  converter which is used
     to convert NO  to NO.                           X
                  x
2.0  TEST ARTICLE DESCRIPTION
     2.1  Chemiluminescent analyzer with a converter capable of transforming
          nitrogen dioxide to nitric oxide.  The nitric oxide is mixed with
          ozone to form an excited state of nitrogen dioxide which emits
          light.  The light energy emitted is then sensed by a photomulti-
          plier tube into an electric current that is nearly proportional
          to the amount of nitric oxide present in the sample.

          o    Thermo Electron  (TECO) Model 10A

3.0  REFERENCES

     3.1  Federal Register, Vol. 39, No. 101, - May 23, 1974.  85.075-23.

     3.2  EPA, Ann Arbor, Preventive Maintenance Guidelines, Appendix B.

     3.3  Matheson Gas Book, "Nitric Oxide Handling Provisions"

4.0  REQUIRED EQUIPMENT

     4.1  NO  Converter Efficiency Detector (see Figure 4-1).
                         C; or AH
                         SUPPL1
                                                CJ"
                Figure 4-1.  NO  CONVERTER EFFICIENCY DETECTOR
                               X
     4.2  NO/N  gas supply, 150 to 250 ppm.

     4.3  O2 or air supply.
                                        109

-------
REVISIONS:

NO EFFICIENCY CHECK
V
TEST
PROCEDURE
PROCEDURE NO.
TP-303
PAGE 3 OFJ 	
5.0  PRECAUTIONS

     5.1  Nitrogen Oxides are TOXIC gases.  Precautions should be taken
          to insure a safe testing environment is maintained.

     5.2  Ozonator should not be pressurized above 10 psig.

6.0  VISUAL INSPECTION

     6.1  Insure the test equipment set up is correct, (see diagram 4.1)

     6.2  Check NO/N  and 0  regulator settings @ 10 psig.
                    ^      ^

7.0  TEST ARTICLE PREPARATION

     See Figure 4-1 for preparation clarification.

     7.1  Connect the NO/N  supply at fitting C2.

     7.2  Connect the O  or air supply at fitting Cl.

     7.3  Attach the analyzer inlet connection to the efficiency
          detector at C3.

               NOTE:   Better response is obtained if detector is plumbed
                      to the normal span gas connection,  rather than
                      the bag connection.
                                      110

-------
REVISIONS:
                             NOy EFFICIENCY CHECK
                           TEST    PROCEDURE
                                                  PROCEDURE NO.
                                                  	TP-303

                                                  PAGE_4_OF _£_
 8.0  TEST PROCEDURE
      The following steps are to be performed to assure an accurate check of
      the converter efficiency.
 Test Sequence
      101
                 Test Description

With the efficiency detector variac in the off
position, place the NOX converter in the bypass
mode and close valve V3.
Data output
      102
      103
Open valve MV2 until stable  flow and readings
are indicated at the analyzer.

Zero the analyzer and set  span output to indi-
cate the NO concentration  being used.  Record
the concentration.
Cone.,  ppm (1)
      104
Open the C>2 flow control  valve  (V3) and adjust
the 02 metering valve (MV1)  to  lower the NO
concentration by 10 percent.  Record the con-
centration.
Cone.,  ppm (2)
      105
Turn on the ozonator and slowly  increase its
voltage until the NO concentration is reduced to
roughly 20 percent of the reading in step 103.
Record this concentration.
Cone.,  ppm (3)
      106
When a stable reading is  obtained from
Step 105, place the NOX converter in the
convert mode.  The analyzer will indicate
the total NOX concentration.  Record the
concentration.
Cone.,  ppm (4)
      107
Turn off the ozonator and allow the analyzer
reading to stabilize.   This  reading is the
NOX concentration of the  dilute span gas.
Record concentration.
Cone.,  ppm (5)
      108       Close valve V3.   The NO concentration should
                be equal to or greater than  the reading in
                Step 103 indicating if the NO/^mixture contains
                NO0.
                                                 Cone.,  ppm (6)
      109       If values do not appear to be  stable or consistent,
                repeat the sequence two or more times.

      110       Disconnect the detector and  restore the ana-
                lyzer to normal operating condition.
                                       Ill

-------
REVISIONS:

NO EFFICIENCY CHECK
v
TEST
PROCEDURE
PROCEDURE NO.
TP-303
PA^F 5 OF 5
 9.0 DATA INPUT

     9.1  Check data sheet for complete and reasonable data.

     9.2  Submit data form #303-01 for analysis

10.0 DATA ANALYSIS

     10.1 Analysis of the converter efficiency is accomplished by the
          NOXCK:SAQE computer program.

     10.2 The efficiency is calculated by substituting the concentrations
          obtained during the test into the following equation as a quick
          check prior to computer analysis.
                                  ". —  I H~ "T  TTl
                                       |_  (c-d)J
% Eff.  =   1+ -^H x 100
          Where:    a = Cone, of Step 106
                    b = Cone, of Step 107
                    c = Cone, of Step 104
                    d = Cone, of Step 105

11.0 DATA OUTPUT

     11.1 Data format with calculation of the percentage efficiency of NO
          converter.                                                     x

12.0 ACCEPTANCE CRITERIA

     12.1 The efficiency of the converter should be above 90 percent.

13.0 QUALITY PROVISIONS

     13.1 If the efficiency of the converter is less than 90 percent, the
          Q.A. department should immediately determine the probable cause
          'for the failure.

     13.2 The complete procedure should be repeated with a new converter
          temperature setting.
                                      112

-------
                                   NOY CONVERTER EFFICIENCY '
                                DETERMINATION - TEST DATA SHEET







PREVIOUS
TEST MO.


-
























DATE


-


-






otr
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	 1
«3.
^

—
I —
-












ANALYZER
VENDOR











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SCALE
RANGE
(PPM)




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CONG.
(PPM)









OPR.
INIT.












BARO
("HG)








CONV.
TEMP.




BYPASS
FLOW
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{SCFH




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GAIN









SETTINGS

ZERO











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,1
          10!
70!
30|
J5|
40|
so!

H
|. .1
uo



c
rr
a:
0
0
0
1
•?
3
TEST SEQUENCE ANALYZER READINGS

(1)










-<





(2)









i| 10






(3)









n






Cf)









30






(5)









75






(6)









30






VARIAC
SET
POINT









35















COMMENTS :





40















45















JO















55















to















«,















70















7i











i
to
 TEST  SEQUENCE CODES;

 (1),   FLOW NO/N2, OZONATOR OFF,  CONVERTER
       BYPASSED

 (2)   FLOW NO/N2 + 02, OZONATOR OFF,
       CONVERTER BYPASSED  (80% OF (1))

 (3)   OZONATOR ON, ADJUST TO GET ABOUT
       10%  OF (1), CONVERTER BYPASSED
Q$'OI*73
 «
  _•

      form 303-01
                           (4)   SWITCH TO CONVERTER MODE

                           (5)   OZONATOR OFF/ CONVERTER MODE

                           (6)   02  OFF, OZONATOR OFF, CONVERT MODE
                                (6)  SHOULD BE GREATER THAN OR EQUAL
                                TO  (1).

-------
EPA TEST
PROCEDURE Um 6r TP-304
Page 1 of 5
SUBJECT
CARBON DIOXIDE AND WATER INTERFERENCE
CHECK FOR THE NDIR CARBON MONOXIDE ANALYZER
Reference FEDERAL REGISTER, VOL 38, November 15, 19
85.075-23. (a) (1) (Hi)
Responsible Organization
CORRELATION AND MAINTENANCE
Test Witness /Review
TEAM LEADER, QUALITY ASSURANCE
Type of Test Report
INITIAL EQUIPMENT CHECKOUT OR WEEKLY CHECK
Report Distribution QUALITY ASSURANCE, CORRELATION ,
MAINTENANCE, TEST OPERATION
73, Data Form No.
Computer Program
NONE
Performance Interval
See Below
Supersedes
New
WD Superseded by
REMARKS/ COMMENTS
1. If the CO-NDIR meets the requirements of 85.075-20 (C) (11) without the
conditioning columns the test is performed to demonstrate conformance to
the criteria when the instrument is first put into service. '
2. If the instrument does not meet the above criteria conditioning columns
must be used and checked weekly or as determined by average column life.
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Branch
Lab Branch



Change
Letter
Section Sigr
Quality Assurance
Test Operations Chief
Support Oper Chief


REVISIONS
Description of Change

lature





Date






Approval

Date

115

-------
REVISIONS--

co /HO INTERFERENCE CHECK
NDIR-CO
TEST PROCEDURE
PROCEDURE NO.
TP-304
PAr.P 2 OF 5
1.0  PURPOSE

     To establish conformance with the interference requirements of
     85.075-20(c)(11) with new instrument trains or to assure the proper operation
     of those trains requiring conditioning columns for removal of CO  and
     water vapor.

2.0  TEST ARTICLE DESCRIPTION

     The carbon monoxide analyzers are of the non-dispersive infrared type.
     Certain instruments available from vendors employ an internal optical
     filtering mechanism to eliminate the interference from CO  and water vapor.

     Instruments that are not free of interference must use sample conditioning
     columns consisting of calcium sulfate or indicating silica gel to remove
     water vapor and ascarite to remove carbon dioxide.

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, Nov 15, 1973  85.075-23(a)(7)(iii)
          Federal Register, Vol. 39, No. 101, May 23,1974  85.075-20(c)(11)

4.0  REQUIRED EQUIPMENT

     4.1  Gas bubbler, sized for the flow rate used for the interference check.

     4.2  Calibration gas, 3 percent carbon dioxide in nitrogen.  Make tolerance
          on the blend should be within ±5% and the analysis for CO  ±2%.  When
          ordering this blend the concentration of the CO impurity should be
          requested not to exceed 1 ppm and/or determined by receiving inspection.

     4.3  Zero Air

     4.4  Zero Nitrogen

     4.5  A portable manifold with selector valves for introducing the above gases
          individually, wet and dry.

     4.6  A hopcolite filter for removing CO from the zero air to establish a
          true instrument zero.

5.0  PRECAUTIONS

     5.1  If a glass bubbler is used it should not be subjected to pressure
          above 2 PSI.

     5.2  The bubbler should be contained or shielded to protect the operator
          in case of explosion (i.e., overpressurization or sudden surge in the
          glass bubbler).
                                     117

-------
REVISIONS:
CO /HO INTERFERENCE CHECK
         NDIR-CO
                          TEST    PROCEDURE
PROCEDURE  NO.
   TP-304
                                              Of
     5.3  Flow rates are important and should be closely  controlled.

     5.4  Extreme care should be taken not to introduce any water droplets or
         aerosol into the train or analyzer.

     5.5  Leak check the manifold before each use by turning off each cylinder
         valve and observing any drop in regulator pressure.

6.0  VISUAL INSPECTION

     6.1  Check ascarite and silica gel columns for color change,
         contamination, and clogging, etc., indicating need for
         replacement.

     6.2  Check water level of  the bubbler.

7.0  TEST ARTICLE PREPARATION

     7.1  The CO analyzer should be on for at least 2 hours prior to test.
                                      118

-------
REVISIONS:
            C02/H O INTERFERENCE CHECK
          	NDIR-CO	

          TEST    PROCEDURE
PROCEDURE  NO.
	TP-304
PAGE_!_OF .5	
  8.0  TEST PROCEDURE
  Test Sequence
       101
       102
       103
       104
       105
       106
       107
               Test  Description
       108

       109


       110

       111
Zero instrument using zero air passed through
the hopcolite to remove the CO using normal train
flow rate and pressure.

Pass zero nitrogen  through instrument to establish
nitrogen zero.  Use this reading for all subsequent
nitrogen zeros.

Span instrument on  lowest range using same flow
rate as zero flow rate.

Repeat nitrogen zero and span until stability
is reached.

Pass zero nitrogen  through water bubbler and
analyzer at  same flow rate.
Bypass water bubbler  and repeat nitrogen zero
Bypass water bubbler  and introduce 3% CO  gas
into instrument.
NOTE:  If CO impurity in the CO  gas is less
that in the nitrogen  the reading may be less
than the nitrogen zero deflection.

Repeat nitrogen zero.

Pass 3% CO  thru water bubbler into instrument
at same flow rate as  the other gases

Repeat nitrogen zero.

Disconnect manifold,  turn off cylinders,  relieve
regulator pressures.
     Data Output
                                                                      Zero
                                                                      Zero & CO
                                                                      Impurity
     Sp n
     Deflection

     Span
     Deflection

     Water vapor.
     deflection
     minus N  zero

     Zero & CO
     Impurity

     Dry CO
     deflection
     Wet CO
     Deflection
                                      119

-------
REVISIONS:
 C02/H20 INTERFERENCE CHECK
           NDIR-CO

TEST     PROCEDURE
PROCEDURE NO.
     TP-304	

PAGE J-OF JL_
  9.0  DATA INPUT

      9.1  Complete form #304-01

  10.0 DATA ANALYSIS

      10.1 Instrument response comparison.

  11.0 DATA OUTPUT

      11.1 Interference  levels for CO  and  HO vapor.

  12.0 ACCEPTANCE CRITERIA

      12.1 The wet CO reading on any range above 300 ppm must be less  than 1% of
           full scale; on ranges below 300  ppm the interference must be less
           than 3 ppm.

  13.0 QUALITY PROVISIONS

      13.1 If the instrument does not meet  acceptance criteria initiate corrective
           action.

      13.2 Repeat the procedure to assure corrective action was successful.
                                     120

-------
             C02/H20 INTERFERENCE CHECK
Analyzer Model 	     Serial #



Date 	       Time
1.       |   |  Zero Instrument




2.  	  Nitrogen zero set point




3.  	  Span deflection  (repeat 2 times)




4.  	  H2
-------
400

-------
Section 400
CORRELATION
      123

-------
  EPA    TEST   PROCEDURE
                                      Number
                            TP-401
                                              Page
                         of
  SUBJECT
 ANALYZER CROSSCHECK
  Reference   EPA, ANN ARBOR, "PREVENTIVE MAINTENANCE
  GUIDELINES."               	   	
                                              Data  Form  No.
                                              401-01	
  Responsible  Organization
 CORRELATION/MAINTENANCE
  Test Witness /Review
 QUALITY ASSURANCE
         CORRELATION/MAINTENANCE LEADER,
                                              Computer  Program
              Performance Interval
              DAILY
  Type of Test  Report
  Report  Distribution
 QUALITY ASSURANCE, TEST OPERATIONS,CORRELATION & MAINTENANCE
                                              Supersedes
                                              NEW	
                                              Superseded by
  REMARKS/COMMENTS
  Office
Program Mgmt
Lab Branch
Lab Branch
Lab Branch
                            ORIGINAL RELEASE APPROVALS
   Section
Quality Assurance
Chief
Test Operations Chief
Support Services Chief
Signature
Date
 Change
 Letter
                                     REVISIONS
 Description of Change
        Approval
Date
                                      125

-------
REVISIONS:


ANALYZER CROSSCHECK
TEST
PROCEDURE
PROCEDURE NO.
TP-401
PAGE_2_OF4 	
1.0  PURPOSE

     To assure the correlation of multiple analyzer trains used for exhaust
     sample analysis.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Gas Analysis System equipped with the following analyzers

          2.1.1     Hydrocarbon - flame ionization

          2.1.2     Carbon monoxide - non-dispersive infrared

          2.1.3     Carbon dioxide - non-dispersive infrared

          2.1.4     Oxides of Nitrogen - Chemiluminescence

3.0  REFERENCES

     3.1  EPA, Ann Arbor, "Preventive Maintenance Guidelines"

4.0  REQUIRED EQUIPMENT

     4.1  Composite bag sample collected from a non-test vehicle or an artificial
          blend from span gases.

5.0  PRECAUTIONS

     5.1  Sample bag should be leak checked.

          5.1.1      (Short method) Fill the bags with background air and draw
                    through the sample system.  If flow indication drops to
                    zero the bags are good, if not replace bag.

6.0  VISUAL INSPECTION

     6.1  Check flow and pressure settings prior to and during bag analysis.

7.0  TEST ARTICLE PREPARATION

     7.1  Perform daily start-up on each system to be checked.

     7.2  Zero and span each analyzer prior to analysis.
                                        127

-------
REVISIONS:

ANALYZER CROSSCHECK
TEST
PROCEDURE
PROCEDURE NO.
TP-401
pAftP 3,OF 4
8.0  TEST PROCEDURE

     The analyzer crosscheck is performed in the following manner.

Test Sequence                 Test Description

     101       Fill a sample bag with enough composite vehicle
               exhaust to perform the crosscheck analysis on' a
               minimum of 4 systems.   (Approximately 3.0 cubic
               feet.)

     102       A representative from Correlation/Maintenance will
               carry the sample to the first train to be checked.

     103       The analyzer operator will analyze the collected
               sample in accordance with the specified analysis
               procedure (TP-707).

     104       The C/M rep. will collect the analyzer traces and
               mark the train number on each trace.

     105       The sample is taken to the remaining trains and
               steps 103 and 104 are repeated for each.
Data Output
                                      128

-------
REVISIONS:

ANALYZER CROSSCHECK
TFST
pporpniiPF
PROCEDURE NO.
TP-401
DAftF 4 OF 4
9.0  DATA INPUT

     9.1  Data is transcribed onto data sheet  #.401-01.

     9.2  A complete set of analyzer traces are collected from each train,
          including the sample concentration.

10.0 DATA ANALYSIS

     10.1 The concentration for each pollutant HC, CO, CO  and NO  is computed
          from the analyzer traces for each train checked by computer program.

     10.2 The concentrations from each train are then compared for any results
          outside of repeatable limits.

11.0 DATA OUTPUT

     11.1 The average values and percent deviation  (if any) of each train.

12.0 ACCEPTANCE CRITERIA

     12.1 Results from the crosscheck should repeat by ±3 percent between each
          system checked.

13.0 QUALITY PROVISIONS

     13.1 if "out of spec" conditions  (see 12.1) exist corrective action will
          be initiated.
                                      129

-------
                                                                          FORM NO.  401-01
ZERO/SPAN DATA
                          ANALYZER CORRELATION DATA SHEET
                                CALCULATED CONCENTRATION
                                                                                   Date:      /     /
                                                                                   Baroireter:	"HG.
DEVIATION

H
(JO
O
Train
NO.
9

15
16
19
21

Gas
Type
HC
CO
C02
NOX
HC
CO
C02
NOX
HC
CO
C02
NOX
HC
CO
CO g
NOX
HC
CO
C02
NOX
HC
CO
C02
NOX
Rge.
NO,
























Cone.
























Set
Point























-- -
Zero
Gain






	








	




	
	


	



	
Span
Gain






	








	




	
	


	



	
Sample
Deflc
























AVERAGE VALUES
HC

























CO

























C02

























NOX

























HC

























• CO

























C02

























NOX

























OPERATOR
~t

.







-------
500

-------
                           Section 500
                           MAINTENANCE
arrently no procedures are included in this section of the manual.
rocedures pertaining to this section must be supplied by the user
nd may be supplied by the EPA in subsequent revisions.
                              131

-------
600

-------
  Section 600
DAILY OPERATION
       133

-------
  EPA    TEST   PROCEDURE
                                      Number
                                             TP-601
                                             Page   i   of _J_
  SUBJECT

OPERATION, MAINTENANCE AND INSTRUMENTATION LOG BOOK  ENTRY  PROCEDURES
  Reference
EPA, ANN ARBOR "PREVENTIVE
                                 LOG BOOK
                                             Data Form No.
                   PQOK
  Responsible  Organization
CORRELATION/MAINTENANCE, TEST OPERATIONS,  INSTRUMENT  SERVICES
                                             Computer Program
                                               NONE
  Test Witness /REVIEW         INST. SERVICES  LEADER
CORR. & MAINT. LEADER. TESTING, TEAM LEADER	
  Type of Test Report
LOG ROOK ENTRY			
  Report  Distribution
Q.A., TEST OPERATIONS, CORRELATION MAINT.,  INST. SERVICES
                                             Performance Interval
                                            DAILY S WHEN NECESSAR'
                                             Supersedes
                                             Superseded by
  REMARKS/COMMENTS
                            ORIGINAL RELEASE APPROVALS
  Office
        MHMT.
LABORATORY BRANC1
LABORATORY BRANC
LABORATORY BRANC
  Section
                 QtTAT.TTY
 CHIEF
 TEST OPERATIONS CHIEF
 SUPPORT SERVICES CHIEI
Signature
Date
                                     REVISIONS
 Change
 Letter
Description of Change
        Approval
Date
                                      135

-------
REVISIONS:


LOG BOOK ENTRY PROCEDURES
TEST PROCEDURE
PROCEDURE NO.
TP-601
PAGE_2_OF J 	
1.0  PURPOSE

     To record all malfunctions, breakdowns and other items related to the CVS,
     Analysis System, and dynamometers that are pertinent in effecting proper
     maintenance and repair of each.

2.0  TEST ARTICLE DESCRIPTION

     2.1  All test and measurement equipment.

3.0  REFERENCES

     3.1  EPA, Ann Arbor, "Preventive Maintenance Guidelines."

4.0  REQUIRED EQUIPMENT

     4.1  Log Book.

5.0  PRECUATIONS

     5.1  Insure that all entries explain the problems/solutions thoroughly.

6.0  VISUAL INSPECTION

     6.1  Log book entries will be checked before each weekly and monthly cali-
          bration/check-out period.

7.0  TEST ARTICLE PREPARATION

     None required.
                                      137

-------
REVISIONS:

LOG BOOK ENTRY PROCEDURES
TEST PROCEDURE
PROCEDURE NO.
TP-601
PAftF 3 OF 4
8.0  TEST PROCEDURE

     In order to make clear, concise log book entries the following steps should
     be followed.
Test Sequence

     101


     102

     103


     104
     105
                                                       Data Output

                                                       Date,  time


                                                       Item
          Test Description

Log the date and time of malfunction or repair
and the responsible technician's initial.

Identify the system or individual equipment item.

In clear terminology state the problem encountered
and repair made.

If the log entry is a malfunction or maintenance
description, log time and date that Correlation/
Maintenance or Instrument Services was notified.
Also identify the person notified.
If the entry is a repair item, state all maintenance   Initials of
performed, and the date and time back on line.  The    responsible
initials of the person responsible for the main-       party
tenance or corrective action should be shown.
                                     138

-------
REVISIONS:

LOG BOOK ENTRY PROCEDURES
TEST PROCEDURE
PROCEDURE NO.
TP-601
PAGF 4 OF 4
9.0  DATA INPUT

     9.1  Record all pertinent items in the appropriate Log Book.

10.0 DATA ANALYSIS

     10.1 A malfunctioning item can usually be diagnosed and repaired more
          efficiently if all aspects of the failure are known.

     10.2 Daily readings of pressure and temperature of the CVS should be checked
          to assure repeatability from day to day.

11.0 DATA OUTPUT

     11.1 Log Book becomes a permanent record of all malfunctions and repair of
          equipment.

12.0 ACCEPTANCE CRITERIA

     N/A

13.0 QUALITY PROVISIONS

     13.1 Entries shall be checked on an audit basis and data compiled
          on all malfunctions and repairs.

     13.2 Frequency of maintenance actions shall be compiled by checking
          the Log Books.

     13.3 Audits of the Log Book will also indicate typical maintenance/repairs
          of test and measurement equipment.
                                     139

-------
INSTRUMENT SERVICES LOG BOOK
                                     TP-601
                                     Attachment No.  1
                  Mm
           Mm
                                  TEC//.
     940757
10 -11-74
                            H-Z9-74
-//-?$
A, A
                 12-7-74

                 12 -9 ~~ 74
           $-7-7^

            '9-7£
     XJ"

     JO
     4AM
                  140

-------
                                                ANALYZER  LOG
DATE
INSTRU. TYPE
GAIN
TUNE
MAINTENANCE/REMARKS
                                                                                                         OPER.

                                                                                                       INITIALS
                                                                                                              rt *a
                                                                                                              ft I
                                                                                                              fo o\
                                                                                                              O O
                                                                                                              (D
                                                                                                              3
                                                                                                              rt

-------
CVS OPERATION LOG
DATE
H
-p-
ro




IN.
PRESS.





OUT.
PRESS.





CVS HOURS





COUNTS :
505





867





505





REMARKS





OPER.
INITIALS

> H
rt TJ
rt .1
(11 
-------
EPA TEST
PROCEDURE Number TP-602
Paae * of 4
SUBJECT
DRIFT/NOISE/GAIN/TUNE CHECKS
Reference
SEE SECTION 3.0
Responsible Organization
CORRELATION/MAINTENANCE, ANALYZER OPERATION
Test Witness/Review
ANALYZER OPERATOR, TEAM LEADER
Type of Test Report
ANALYZER LOG BOOK ENTRY
Report Distribution
QUALITY ASSURANCE, CORRELATION AND MAINTENANCE
Data Form No.
ANALYZER OP LOG BK
Computer Program
NONE
Performance Interval
DAILY
Supersedes
NEW
Superseded by
REMARKS/ COMMENTS
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Branch
Lab Branch
Lab Branch


Change
Letter
Section Signature
Quality Assurance
Chief
Supp Services Chief
Test Operations Chief

Date





REVISIONS
Description of Change Approval

Date


-------
REVISIONS:

DRIFT/NOISE/GAIN/TUNE CHECKS
TEST
PROCEDURE
PROCEDURE NO.
TP-602
PA^P 2 OF 4
1.0  PURPOSE

     To perform a daily check of the analyzers and recorders used in the
     analysis system.

2.0  TEST ARTICLE DESCRIPTION

     2.1  An analysis system equipped with the following analyzers.

          2.1.1  Hydrocarbons - Flame ionization

          2.1.2  Carbon monoxide - NDIR (non-dispersive infrared)

          2.1.3  Carbon dioxide - NDIR

          2.1.4  Oxides of Nitrogen - Chemiluminescence

     2.2  Strip chart recorders

3.0  REFERENCES

     3.1  EPA, Ann Arbor, Training Manual, "Light Duty Certification
          Procedures"

     3.2  EPA, Ann Arbor, "Preventive Maintenance Guidelines"

4.0  REQUIRED EQUIPMENT

     4.1  "Working" span gases

     4.2  Zero air or nitrogen gases

5.0  PRECAUTIONS

     5.1  If any discrepant conditions are observed the analyzer operator
          shall not attempt any repair or adjustment.   The condition shall
          be reported to Correlation/Maintenance and/or Instrument Services
          for investigation and disposition.

6.0  VISUAL INSPECTION

     See Section 8.0

7.0  TEST ARTICLE PREPARATION

     7.1  The instruments shall be warmed up to stable operating conditions
          (as per individual manufacturer's requirements)

-------
REVISIONS:
                           DRIFT/NOISE/GAIN/TUNE CHECKS

                           TEST     PROCEDURE
                                                 PROCEDURE NO.
                                                      TP-602	

                                                 PAGE_2-OF _L.
 8.0  TEST PROCEDURE

      The following steps are to be accomplished to check the efficiency
      of the analyzers and recorders.
 Test Sequence                 Test Description

      101       Zero drift is checked in the  following manner.

       A             o  Introduce zero gas  into the analyzer
                                                      Data Input
       B
       E

      102
      103
      103A
      104
     o  Adjust the analyzer to  read zero
        millivolts and set the  chart
        recorder on zero

     o  Allow zero gas to flow  for approxi-
        mately 5 to 10 min.

     o  From the strip chart determine the
        difference between the  highest and
        lowest value of the zero trace.

     o  Record difference as   C

Excessive noise is indicated on the chart
recorder by signal spiking.
NOTE:  Noise may be caused by the
recorder or the analyzer, therefore the
gain adjustment of the recorder should
be checked.

The gain setting should be checked daily
to assure a major shift has not occurred.
Record the analyzer gain setting and check
reading from following day.  Record percent
change.

If the chart recorder is insensitive or
oversensitive to small changes  in input
signals (0.50% of full scale),  record
the problem in the log book.

If a normal operating span point cannot be
reached, or a negative read-out is indicated
when a span gas is introduced to an analyzer,
record out of tune.   Document the type of
response in the log book.  (Instrument
Services and/or Correlation will make final
decision to the type of problem encountered)
   C

Noise
Gain set.,
% change
Recorder
gain
Out of
tune

-------
REVISIONS:

DRIFT/NOISE/GAIN/TUNE CHECKS
TEST
PROCEDURE
PROCEDURE NO.
TP-602
PAGF 4 OF 4
9.0  DATA INPUT

     9.1  Record any drift, noise, gain or tune problems in the Analyzer
          log book  (attachment A).

10.0 DATA ANALYSIS

     10.1 Determine if the problem recorded is an analyzer or recorder
          malfunction by comparing historical readings in the analyzer
          log book.

     10.2 Determine if the problem is of sufficient magnitude to warrant
          maintenance.

11.0 DATA OUTPUT

     11.1 Enter results in the analyzer log and history file.

12.0 ACCEPTANCE CRITERIA

     12.1 Drift should not exceed ±1% of full scale

     12.2 Noise should not exceed ±1% of full scale

     12.3 Shifts in gain settings should not exceed ±1% in any 24 hour period.

     12.4 Compare readings to those  in the analyzer log.

13.0 QUALITY CONTROL PROVISIONS

     13.1 If problem warrants maintenance submit a corrective action request.

     13.2 Prepare and maintain control charts for future  analysis.

-------
                                                ANALYZER LOG
DATE
     H

     —5
INSTRU. TYPE
GAIN
TUNE
MAINTENANCE/REMARKS
                                                                                                         OPER.

                                                                                                       INITIALS
                                                                                                              rt I
                                                                                                              fa 
-------
EPA TEST
PROCEDURE Number Tp.6Q3
Paqe i of 5
SUBJECT
TEST VEHICLE SCHEDULING
Reference
EPA, ANN ARBOR, PRODUCTION CONTROLLER
Responsible Organization
PRODUCTION CONTROL
Test Witness /REVIEW
•TOST REQUESTOR
Type of Test Report
DAILY AND WEEKLY LOG SHEETS
Report Distribution
REQUESTOR, PRODUCTION CONTROL, LAB SECTION CHIEF
Data Form No.
603-01 thru 07
Computer Program
NONE
Performance Interval
DAILY (
Supersedes
NEW
Superseded by
REMARKS/ COMMENTS
1.0 THIS PROCEDURE IS BEING MODIFIED BY EPA IN CONJUNCTION WITH THE
NEW DATA PROCESSING ROUTINES.

Office
t>nrv-»aM MCMT
TABORATORY BRANCI
LABORATORY BRANH
LABORATORY BRANCI


Change
Letter
ORIGINAL RELEASE APPROVALS
Section Signature
nUALITY ASSURANCE
CHIEF
PRODUCTION CONTROLLER
TEST OPERATIONS CHIEF




REVISIONS
Description of Change

Date






Approval

Date


-------
REVISIONS:

TEST VEHICLE SCHEDULING
TFST ppnrpniiPF
PROCEDURE NO.
TP-603
PAftF 2 |OF 5
1.0  PURPOSE

     To schedule all vehicle testing to be performed by Testing Operations.

2.0  TEST ARTICLE DESCRIPTION

     The vehicle to be tested may be of any type as long as it can be driven
     on a dynamometer, has an engine displacement of at least 50 cubic inches,
     meets the Federal Register requirements for a light duty vehicle and
     meets the criteria of acceptance in test procedure #701.

3.0  REFERENCES
     Procedures Manual Section 5.3

4.0  REQUIRED EQUIPMENT

     None

5.0  PRECAUTIONS
     Does not apply

6.0  VISUAL INSPECTION

     None

7.0  TEST ARTICLE PREPARATION

     None
                                       151

-------
REVISIONS:

TEST VEHICLE SCHEDULING
TEST PROCEDURE
PROCEDURE NO.
TP-603
PAOF,3 .OF5
8.0  SCHEDULING PROCEDURE

     The procedure for scheduling of a vehicle covers the period from the
     initial request thru the final release of the vehicle from the test area.
     Scheduling is done on a daily and weekly basis.  Testing schedule pro-
     jections are done on a yearly basis using information on testing requests
     obtained from Certification and other divisions.

Test Sequence                           Description

     101            All request for tests are sent to Production Control
                    using a form such as 603-04.  See Figure 8.1.

     102            Production control schedules the test and sends verifi-
                    cation of test time and date to the requestor.  For
                    certification tests form #603-03, Job Request, is used.

     103            Production control makes out the test schedule for the
                    week on Thursday and submits the schedule to Testing
                    Operations and the Laboratory Branch Chief using
                    form #603-06.

     104            Confirmation of schedule is returned to Production
                    Control on Friday.

     105            Daily schedules for each test are all submitted to the
                    Light Duty Testing Supervisor on the preceding day
                    using form #603-06.

     106            Weekly schedules are submitted to the Evaluational Devel-
                    opment section on the preceding Friday using form #603-07.

     107            The projected scheduling for the Laboratory Branch is
                    revised and submitted to testing operations and the
                    Laboratory Branch Chief on the first of each month.

     108            Production control receives and ships the vehicle after
                    notification of valid test using form #603-01.  In addition
                    the shipping and receiving order must be authorized by both
                    the EPA Division Representative and the Manufacturers
                    Representative',

                    In cases where the above authorizations are not available
                    the signature of the Laboratory Branch Chief is required.

     109            If the test for any reason is invalid it is rescheduled at
                    the earliest convenient date.  Notification of new time
                    and date is sent to the requestor.
                                      152

-------
REVISIONS:
                      TEST VEHICLE SCHEDULING

                       TEST   PROCEDURE
                              PROCEDURE NO.
                                  TP-603
      TEST
   REQUESTOR
 j  LABORATORY
     BRANCH
      CHIEF
     TESTING
   OPERATIONS
                  Figure 8.1    Scheduling Procedure
     PRODUCTION

      CONTROL
     WORK ORDER
     EACH TEST

      4 COPIES
     PRODUCTION
      SCHEDULE
           ANNUAL
 WEEKLY
          LT. DUTY
          TESTING
                             _v
   DAILY
               .	\L

E. & D.
TESTING
r

HEAVY DUTY
TESTING


                      TEST VALIDATION
              TECH.
EPA REP.
MAN. REP.
                 SHIPPING
                     &
                RECEIVING
                                                       CO
                                                       W
                                                       Q
                                                       H
                                                       3
EH
CO
W
EH
Q
H
^

$
                                 153

-------
REVISIONS:

TEST VEHICLE SCHEDULING
TEST PROCEDURE
PROCEDURE NO.
TP-603
PAGE 5 OF 1 	
9.0  DATA INPUT




     Does not apply.




10.0 DATA ANALYSIS




     None




11.0 DATA OUTPUT




     Does not apply.




12.0 ACCEPTANCE CRITERIA




     None




13.0 QUALITY PROVISIONS




     13.1 Forms and procedure reviewed by Quality Assurance Management.
                                      154

-------
                                        UNITED STATES
                            ENVIRONMENTAL PROTECTION  AGENCY
                                        2565 Plymouth Road
                                     Ann  Arbor,  Michigan 48105

                              SHIPPING  AND  RECEIVING ORDER
Manufacturer
Identifying No.(s)
                        CD
                        (5)
                       ®
CD
Description, Special Marks, and Exceptions
        The vehicle/engine(s) described above was/were  RECEIVED into custody of this installation on
                          19	 at	 AM  	PM.
   D  The vehicle/engine(s) described above is/are officially RELEASED to the manufacturer or his representa-
 tive on	 19	  at	 AM  	  PM.
                                                  EPA Division Representative
                                                   D CSD      D ECTD      C3 AAPSD
                                                  Manufacturer Representative
                                                  Production Control Office
 Date
           AM
PM
                         Received by
 EPA (XAA-JOJ) 8-74
                                           FORM #603-01
                                                   155

-------
MSPCP(AA) 3-10-73
REQUEST
  Name _
   LABORATORY BRANCH
COMPLIANCE TEST REQUEST
  Section
                                       Job #_

                              Date Submitted .
                                    Extension _
  Test Type: Q Data     Q Correlation     D 2nd Retest
            D.Durability     D 1st Test                     Reason:.
            n Running Change    Qlst Retest	
  Test Procedure .	
  Special Test(s) Requested.
  Description:
    Manufacturer	
    Identification	
    Engine Family
    Reference No.
  Expected Delivery Date
  Latest Acceptable Completion Date
SCHEDULE
  Prep Date	
  Test Date	
Production Controller's Comments:
LD.
                         H.D.
                       System
              RESCHEDULED FOR
             .  Delivery Date	
             .  Prep Date	
                Test Date	
                                                                         Job #.
Requestor
TEST TEAM REPORT
Date Receiver)
Comments
TECHNICIAN REPORT
Date Regan
Date Hnmplete
Cnnriment«;/Prnhlem<;

Section Fxt.
Technician Assigned

Time arn/pm Man-Hours
Tirne am/pm




TEST VALIDITY
FPA Rep,
Technician
Manufacturer1? Rep.
|f invalid, why?

D Valid n Invalid
D Valid Q Invalid
D Valid n Invalid


                                        156
    FORM #603-02
              WHITE: REQUESTOR'S COPY
              YELLOW: PRODUCTION CONTROLLER'S COPY
              PINK: LAB SECTION CHIEFS COPY
              GOLDs REQUESTOR'S IN-PROCESS COPY

-------
MSPCP(AA) 1-10-73                   LABORATORY BRANCH
                                       JOB REQUEST
                                                                      Job #.
REQUEST
  Name .	Date Submitted .
  Branch	Section	Extension
  Project Number/Description 	
  Job Description (Attach sketches needed)
  Special Equipment Required	
  Proprietary Item:  n Yes   Q No
  Craft Requested	
  Date Item To Be Delivered for Test	
  Latest Acceptable Completion Date	
  SCHEDULE                                   RESCHEDULED FOR
    Date Request Rec'd	    Date	Time	am/pm
    Craft(s)/Team Assigned	    Reason	
    Date	Time	am/pm
                                                                      Job #.
Requestor	 Branch	 Ext.
  CRAFT/TEAM REPORT
    #1  	    #2  	
    Technician 	    Technician 	
    Date Began	Time	am/pm    Date Began 	Time 	am/pm
    Date Complete	Time	am/pm    Date Complete	Time	am/pm
    Man-Hours 	    Man-Hours 	
    Comments/Problems  	    Comments/Problems  	l_
    FORM #603-03
                                             WHITE: REQUESTOR'S COPY
                                             YELLOW: PRODUCTION CONTROLLER'S COPY
                                             PINK: LAB SECTION CHIEFS COPY
                                             GOLD: REQUESTOR'S IN-PROCESS COPY

-------
                                           ADVANCE TEST PROJECTION REQUEST
                                       DIVISION OF CERTIFICATION AND SURVEILLANCE
H
GO
Projection Period
Manufacturer
Name

•








Name
Identification
Number










Delivery
Date










Test-
Date










Branch/ Section Extension Date Submitted
Requirement
" Indicate Year Eclowf'72. '73. '74. '75. '76. '77. '78. '79. '801
emission
Data
A










Correlation
B










Durability
c










Surveillance
D










Running
Change
E










Total











Other (Specify)
F










FORM #603-04

-------
          Period
LIGHT^DUTY TESTING  SCHEDULE


                      Date Submitted
Test
Time











Sun.
Name/ID











Mon.
Name/ ID



*







Tues.
•Name/ID











Wed.
Name/ID











Thurs.
Name/ID











Fri.
Name/ ID











Sat.
Name/ID











H
vn
          FORM #603-05

-------
                    ENVIRONMENTAL  PROTECTION AGENCY
                         Office.of Air  Programs
                      Ann Arbor,  Michigan  4S105
Light Duty Testing Schedule
Date
Submitted

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-------
                 ENVIRONMENTAL PROTECTION AGENCY

                    Ann Arbor, Michigan 4S105
E § D   Testing Schedule for
Date
Submitted
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                               161

-------
EPA TEST PROCEDURE
SUBJECT
DYNAMOMETER WARM-UP/SET
Reference Federal Register, Vol. 36
October 31, 1973, Sec. 85.075-15
Responsible Organization
Test Operations
Test Witness /Review
Team Leader
Type of Test Report
Data Sheet
TP-604 page I Of 4

J» NO. 209 Data Form No.
705-01
Computer Program
Performance Interval
Daily
Supersedes
New
Report Distribution Superseded by
O.A. . Data Validation. Certification Branch
REMARKS/COMMENTS
ORIGINAL RELEASE APPROVALS
Office Section
Pj-^ijrgm MciTjnvt "^ualit" Assurance
Laboratory Branch Chief
Signature


Laboratory Branch Test Operations Chief



Date





REVISIONS
Change
Letter Description of Change Approval

Date

163

-------
REVISIONS:

DYNAMOMETER WARM-UP
TFST PPOrFHIIPF
PROCEDURE NO.
TP-finA
PAGE_2_OF JL-
1.0  PURPOSE

     To assure the Dynamometer and associated equipment has been conditioned
     properly.  The horsepower/inertia for first vehicle is also set at this
     time.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Chassis dynamometer having the capabilities described in Federal
          Register 85.075-15.

     2.2  Associated speed and horsepower (torque) meters.

     2.3  Drivers Aid, Varian or Hewlett-Packard.

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 209 - Oct. 31, 1973 - Sec. 85.075-15

     3.2  EPA, Ann Arbor, "Light Duty Test Operations", Draft

4.0  REQUIRED EQUIPMENT

     4.1  Light-weight non-test vehicle

5.0  PRECAUTIONS

     5.1  Check carefully to assure that the desired Hp and Inertia is properly
          set.

     5.2  Inflate tires to 45 psi, to protect against blow-outs

     5.3  Tie down vehicle with winch cable.

6.0  VISUAL INSPECTION

     6.1  Check the vehicle alignment on the dynamometer

7.0  TEST ARTICLE PREPARATION

     7.1  Drive non-test vehicle onto dynamometer

     7.2  Check "drivers-aid" for paper, ink and zero calibration

     7.3  Position cooling fan within 12 inches of vehicle radiator, to prevent
          overheating

     7.4  Insure vehicle exhaust is properly vented
                                       165

-------
REVISIONS:
                         DYNAMOMETER WARM-UP
                           TEST    PROCEDURE
PROCEDURE  NO.
    TP-604
PAGE_3__OF
 8.0  TEST PROCEDURE

     The following steps are  to be performed for proper dyno  warm-up and horsepower
     setting.

 Test Sequence            Test Description                            Data Output

     101       Prior to the first test of the day, drive
               warm-up vehicle at 30 mph for 15 minutes

     102       Stop vehicle,  set inertia weight and select           Inertia Wt,
               horsepower required for next certification            Ibs. indi-
               vehicle to be  tested.  Record inertia wt.  and          cated
               Hp. in Section II of form #705-01.                    horsepower

     103       Accelerate to  50 mph; using the loading
               control switch set Hp required for next vehicle
               (Automatic loading system may be used).

     104       Hold steady at 50 mph/or 5-minutes.  Check
               calibration of the "drivers-aid" against the
               speed meter to assure they both indicate
               50 mph.  If the drivers-aid is out of ad-
               justment contact the Team Leader.

     105       Stop the warm-up vehicle disconnect ex-
               haust vent system and remove the vehicle from
               the dynamometer.
                                     166

-------
REVISIONS:

DYNAMOMETER WARM-UP
TFST
ppnrpniiPF
PROCEDURE NO.
TP-604
RAftF 4 OF 4
9.0  DATA INPUT

     9.1  Complete Section II of data form #705-01.

     9.2  Technician will sign and date form when warm-up is complete.

10.0 DATA ANALYSIS

     None Required

11.0 DATA OUTPUT

     11.1 Form #705-01 will remain with cert, vehicle until completion of DE-PREP -

12.0 ACCEPTANCE CRITERIA

     12.1 Correct inertia and horsepower setting must be indicated in Section II
          of form #705-01.

     12.2 Check for signature of Technician, indicating warm-up and horsepower
          set was performed.

13.0 QUALITY CONTROL PROVISIONS

     13.1 Any equipment malfunctions (i.e., drivers-aid, dyno,  meters)  will be
          reported to Q.A. department by the Team Leader or Test Operations
          representative and corrective action (maintenance)  should be
          initiated.
                                     167

-------
                    VEHICLE TEST AND  EVAPORATIVE DATA

Vehicle Mfgr.	   . _:	 No.
Inertia

Wt. HP A/C Test

I. HEAT -BUILD

A
B

C

D

E

F
G

H

I

J

K

L

M

. Drain fuel
. Plumb air cleaner

. Plumb canister

. Plumb bowl vent (if required)

. Trap gas cap (if required)

. Seal orifices/vents
. Install carbon traps (record on data sheet)

. Hook-up temperature recorder

. Hook-up thermocouple leads

. Install heat blanket
1
. Plug in fuel tank heater (when used)

. Refuel vehicle - 40% of tank capacity
Tech. Sig. Witness Sig.
. Replace fuel cap, plug exhaust pipe(s) Unclamp
H

TECH
D

D
D
-"
D

D

D

D
D

D

a

a

a


canister Q


CTA
D

D
D

a

a

a

a
a

a

a

a

a


a
      Heat Build  Fuel Temp.   Fuel Temp.  Ambient
       Progress   Lead No.  1   Lead No.  4    Temp.

        0-Min.    	   	  	

       15-Min.    	   	  	

       30-Min.    _^	   	  	

       45-Min.    	   	  	

       60-Min.
II.   DYNAMOMHTF. R WARM - IIP/ S P.T

     A.  Drive non-test vehicle onto dyno  B. Hook-up vehicle  as  for Hot LA-
     C.  Set inertia	ibs.Q	II.P.  D. Drive @50mph  steady state
     h.  Remove vehicle from dyno
 I.   Tech.  Sig.	'                       Date
II.   Tech.  Sig.
                                                    Date
  FORM 705-0]                       168

-------
700

-------
   Section 700
EMISSION TESTING
       169

-------
EPA TEST
SUBJECT
TEST VEHICLE
PROCEDURE NU'
nber
TP-701 Page i of 4
INSPECTION AND ACCEPTANCE
Reference EPA Trainin9 Manual, "Light
Procedures"
Responsible Organization
Production Control
Duty Certification Data porm No
701-01
Computer Program
None
Test WitneSs/Review Performance Interval
Manufacturer's Representative, Certification Rep., Q.A. See Comments
Type of Test Report
Data Sheet
Supersedes
New
Report Distribution Superseded by
Q.A. , Data Validation, Certification Branch
REMARKS/ COMMENTS
Each vehicle must be inspected and accepted prior to each emission test.
ORIGINAL RELEASE APPROVALS
Office
Program Man.gmt .
Laboratory Branch
Laboratory Branch


Section
Quality Assurance
Chief
Test Operation Chief


Signature





Date





REVISIONS
Change
Letter
Description of Change
Approval

Date
I
i
|
171

-------
REVISIONS:
                    TEST VEHICLE INSPECTION AND ACCEPTANCE
                           TEST    PROCEDURE
PROCEDURE NO.
PAGE_2_OF
 1.0  PURPOSE

     To determine whether a vehicle is properly prepared and acceptable for
     emission testing, each vehicle will be inspected prior to vehicle
     preparation.

 2.0  TEST ARTICLE DESCRIPTION

     Test vehicle meeting manufacturer's and Federal requirements.

 3.0  REFERENCES

     EPA, "LIGHT DUTY CERTIFICATION PROCEDURES," TRAINING MANUAL, APPENDIX

 4.0  REQUIRED EQUIPMENT

     None required

 5.0  PRECAUTIONS

     5.1  If a vehicle being inspected does not have  a  required device, the
          team leader should be contacted.

 6.0  VISUAL INSPECTION

     SEE "TEST PROCEDURES."

 7.0  TEST ARTICLE PREPARATION

     7.1  PREPARED BY VEHICLE MANUFACTURER.
                                     173

-------
REVISIONS:
                   TEST VEHICLE INSPECTION AND ACCEPTANCE

                           TEST    PROCEDURE
                                                  PROCEDURE NO.
                                                     TP-701	

                                                  PAGE_L-OF JL-
8.0  TEST PROCEDURE

     The following inspection must be followed for proper vehicle acceptance.
Test Sequence

     101


     102

     103

     104

     105


     106


     107


     108

     109


     110

     111
            Test Description

Check vehicle  for valid license  plate,  properly
mounted.

Check for exhaust adaptor

Is fuel drain  connected

Thermocouple lead hook-up

Vehicle Damage, note on back of data sheet


Insure equipment is connected (notify production
control if disconnected equipment is found)

Insure manufacturer's data sheet is clearly
posted.

Check oil level  (if low, notify production control)

Check for minimum 1/4 tank fuel level (add if
required).   NOTE:  See Vehicle Fueling  Procedure.

Check for manufacturer's start-up procedure.

If the above data is complete clear for AMA route.
Data Output

OK, NONE


OK, NONE

OK, NONE

OK, NONE

OK, NOTE
ON BACK
OK, NONE


OK, NONE

OK, NONE


OK

OK

-------
REVISIONS:


TEST VEHICLE INSPECTION AND ACCEPTANCE
TEST
PROCEDURE
PROCEDURE NO.
TP-701
PAftF 4 OF 4

 9.0 DATA INPUT

     9.1  Submit completed Inspection form #701-01 to Data Validation following
          evaporative testing.

10.0 DATA ANALYSIS

     10.1 Insure all required information is complete and correct.

11.0 DATA OUTPUT

     11.1 Data form 024-01 submitted to Certification Branch for vehicle file
          storage.

12.0 ACCEPTANCE CRITERIA

     12.1 Vehicle must follow criteria stated in Section I of Driver's
          Preconditioning form.

13.0 QUALITY CONTROL PROVISION

     13.1 If vehicle is not within acceptable limits the manufacturer's repre-
          sentative should be notified prior to "AMA" preconditioning.

     13.2 The inspector shall verify all conditions have been satisfied and shall
          enter his EPA I.D. # on the vehicle test data sheet.
                                      175

-------
 Vehicle mfgr.
 F.T.P. MINUS EVAP PLUS F.E.T.

DRIVER'S PRECONDITIONING REPORT


                      No.
Time Out Time In
Date
I. VEHICLE INSPECTION
A. Valid License Plate
B. Exhaust Adaptor
C. Fuel Drain
D. Vehicle Damage
Odom



Testft
D
D
D
a
OK
OK
OK
OK
D
a
a
a
None
None
None
Note
F.
G.
H.
I.
Mfgr
's Data
Sheet
Oil level; if low
notify Prod. Cont.
Odom Reading
Fuel
level.
1/4-
DOK
DOK
a OK

DNone
D Note

         (note on reverse)

     E.  Equip, not con-
         nected notify
         Prod. Cont.
                Note
   tank min,; add if
   required.

J. Start-up per Mfg. DOK
   instructions

K. Drive AMA route   DOK
II.   AMA PRECONDITIONING

     A.   Engine Start

     B.   Ignition Switch

     C.   Starter Motor

     D.   Fast  Idle

     E.   Transmission

     F.   Clutch

     G.   Brakes

     H.   Driveability
     DGood          D Hard

     DOK            D Other

     D OK            D Grinds

     D OK            D None

     D OK            D Shifts Hard

     D OK     Grabs  D Slips

     D OK     Fade   D Poor
               D False



               D No Start

               D Engine Hot



               D N/A

               D None
     D Surge  DStumble  DBack Fire  D Stretchy
       Engine Miss D       DieselsD
     D OK
    Driver's  Signature
                                   176
   FORM 701-01

-------
  EPA    TEST   PROCEDURE
                                      Number
                            TP-702
                                                               Page
                         of  7
  SUBJECT

 EVAPORATIVE EMISSIONS PREPARATORY PROCEDURES
  Reference  FEDERAL REGISTER, VOL.  38, NO.  209, Oct. 21,
 	85.075-11  S EPA TRAINING MANUAL	
                                        1973
  Responsible Organization
 TEST OPERATIONS
  Test Witness/Review
 TEAM LEADER, QUALITY ASSURANCE
  Type of Test  Report
 DATA FORM OUT-PUT
  Report  Distribution
 QUALITY ASSURANCE, DATA VALIDATION, TEST FILE, CSD
              Data  Form No.
               701-01
                                              Computer Program
                                                               NONE
                                              Performance  Interval

                                              PER CERT.VEHICLE
                                              Supersedes
                                             JNEW		

                                              Superseded  by
  REMARKS/COMMENTS
                            ORIGINAL RELEASE APPROVALS
  Office
Program Mgmt
Lab Branch
Lab Branch
   Section
Quality Assurance	
Chief
Test Operations Chief
Signature
Date
 Change
 Letter
                                     REVISIONS
 Description of Change
        Approval
Date
                                     ITT

-------
REVISIONS:

EVAPORATIVE EMISSIONS
PREPARATORY PROCEDURES
TFST PPOrFHIIPF
PROCEDURE NO.
TFr-702
PAGF 2 OF 7
1.0  PURPOSE

     To prepare test vehicles for the Diurnal (Heat Build) Evaporative test
     and the 1975 FTP.

2.0  TEST ARTICLE DESCRIPTION

     Test vehicle (see Section 5.0 below)

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 209, Oct 21, 1973, Para. 85.075-11

     3.2  EPA, "Light Duty Certification Procedures," Training Manual.

4.0  REQUIRED EQUIPMENT

     4.1  Engine analyzer which includes:
          NOTE:  See manufacturer's manual for calibration procedure.

          o    Timing light
          o    Tachometer
          o    Dwell Meter

     4.2  CO Analyzer (i.e., Mexa 300, Sun, Snap-On,  etc.)
          (Calibrate as shown in manufacturer's manual)

     4.3  Chassis dynamometer (see procedure #202 for calibration.)

     4.4  Variari, "driver's aid" (see procedure #204  for calibration

5.0  PRECAUTIONS

     5.1  If the following items are not on the vehicle  Dp_ Not Continue Test!

          o    Vehicle test data sheet
          o    Marmon coupler
          o    Evaporative plumbing
          o    Thermocouples
          o    Fuel drain

     5.2  If the vehicles has to be weighed, lock the scale platform before
          moving vehicle on or off.

     5.3  Use the proper fuel for each vehicle (see procedure #704)

     5.4  When driving the "A.M.A." route, insure conditions are safe  and
          do not exceed the speed limit.  If road conditions are UNSAFE
          return to garage by shortest route.

     5.5  Do not do any maintenance or adjustments and do not hook up any
          disconnected devices.
                                      179

-------
REVISIONS:

EVAPORATIVE EMISSIONS
PREPARATORY PROCEDURES
TEST PROCEDURE
PROCEDURE NO.
TP-702
PAGE 3 OF_1_
     5.6  If vehicle does not start inform supervisor and manufacturers
          representative.

     5.7  Be sure the "AMA" route has been driven prior to the LA-4.

     5.8  If vehicle does not have sufficiently good drivability to follow
          LA-4 trace, report to the Team Leader.

6.0  VISUAL INSPECTION

     6.1  Insure basic preliminary data is clearly posted  on the vehicle.

     6.2  Carefully inspect for disconnected devices.

7.0  TEST ARTICLE PREPARATION

     7.1  Obtain car keys from the Production Controller.

     7.2  Obtain the Preconditioning Driver's Report form  #701-01
                                      180

-------
REVISIONS--
                         EVAPORATIVE EMISSIONS
                         PREPARATORY PROCEDURES
                           TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                     TD—7/19
                                                 PAGE-d— OF
  8.0   TEST PROCEDURES

       The following steps must be taken to insure the proper preparation  of
       a  test vehicle for the 1975 Evaporative Emission and Federal  Cycle
       Test.
  Test Sequence
       101
       102
       103
            Test Description

Fill out vehicle condition section of  form
701-01 (Preconditioning Drivers  Report)

Insure that colored tape is attached to steering
wheel/fuel cap and data sheet.   (Red or Orange
= indolene clear)  (green = indolene 30)

Start the vehicle according to manufacturer's
procedures.  Check the following items on the
engine start section of the preconditioning
driver's report, with an "x."

o    Satisfactory engine start
o    If engine cranks for 10 seconds or more
o    If engine starts and then dies/record
     number of false starts
o    Check seat belt interlock function
       103A     o     Ignition switch satisfactory
                o     Ignition switch fails

       103B     o     Starter motor engages properly
                o     Starter motor grinds
                o     Starter malfunctions
Data Output

Form Require-
ment
                                                                  Good
                                                                  Hard Start
                                                                  False start
                                                 Okay
                                                 Other

                                                 Okay
                                                 Grinds
                                                 Other
       103C      o    Car starts and fast idles without stalling
                o    Car starts but does not fast idle
                o    Car has been driven immediately prior to
                     start  (fast idle not required)
       104       Weigh vehicle at designated area.  Record on
                checksheet
                                                 Okay
                                                 None
                                                 Engine Hot

                                                 Curb Weight
       105       Check for fuel level.  If less than 1/4 full,
                take the vehicle to area designated for
                fueling  (note;  check for type of fuel needed
                by color tape)

       105A      If fuel is added record the date, fuel type
                and amount on "vehicle test fuel record."
                This must be signed by the technician and  a
                witness.
                                                 Date
                                                 Fuel Type
                                       181

-------
REVISIONS:
                          EVAPORATIVE EMISSIONS
                          PREPARATORY PROCEDURES
                           TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                 PAGE.S—OF
 Test Sequence

      106



      106A



      107


      107A
            Test Description

Drive the "A.M.A." preconditoning route.  (See
Attachment A to  this procedure.)  Note depart-
ing time on drivers form.

After completing the AMA route, log in time
and take the vehicle to the designated
prep bay

Evaluate drivability.  If the vehicle drives
well, indicate good on checksheet

If the vehicle does not drive well check
"other" and evaluate criteria listed below
Data Output

Date/Time
Date
Time
Good
Other
                             Transmisssion
      107B      o    Transmission smooth

                o    Transmission (manual)  difficult to
                     operate

                o    Transmission (automatic)  jerks between
                     shifts

                                Clutch

      107C      o    Clutch operates smoothly

                o    Clutch grabs, slips or malfunctions

                o    Automatic transmission indicate "N/A"
                     in other space

                                Brakes

      107D      o    Brakes function properly

                o    Brakes grab, fade, squeal or malfunction

      108       If vehicle pulsates when driven at a constant
                speed, indicate surge

      108A      If vehicle has a short, sharp reduction in
                acceleration rate, indicate stumble
                                                 Shifts  hard
                                                 Shifts  hard
                                                 Okay

                                                 Other

                                                 N/A
                                                 Okay

                                                 Other

                                                 Surge


                                                 Stumble
                                      182

-------
REVISIONS:
                          EVAPORATIVE EMISSIONS
                          PREPARATORY PROCEDURES
                           TEST     PROCEDURE
                                                  PROCEDURE  NO.
                                                     TP-702	

                                                  PAGE_§_OF 2	
 Test Sequence
      108B
      108C
      108D
      109
      110
      110A
      HOB
      HOC
      HOD

      HOE


      HOP

      HOG

      111
            Test Description

 If  the vehicle has a lack of anticipated
 throttle response, during light/moderate
 accels, indicate stretchy

 If  any loud popping noises are detected
 coming from the tailpipe or carburetor,
 indicate backfire

 If  the engine continues to run when ignition
 is  turned off, indicate diesel

 Following the evaluation steps listed  above
 the driver must sign his name to the form

 The following steps must be taken and  infor-
 mation recorded on the Vehicle Inspection
 section of the preconditioning drivers
 report.

 Check the idle CO using an infrared
 analyzer such as a Mexa 300.   Check/adjust
 the calibration settings.

 Follow the method for checking timing  posted
 on  the vehicle data sheet  (should be posted
 in  window of vehicle)  check the timing and
 record under "Measured Values."

 Insure that reading taken  is within accept-
 able tolerance allowed by  EPA.   If out of
 tolerance contact supervisor and manufacturers
 representative

 Record RPM at which timing was taken

 Check idle RPM (use manufacturer's tech-
 nique)  and record.   Check  tolerance.

 Check and record tire  size

Check axle ratio or N/V

 Record date and the technician must sign
 this form
Data Output

Stretchy



Backfire



Diesel


Signature
                                                                % CO
                                                                Degrees
                                                                before or after
                                                                TDC
RPM

RPM


Tire Size
Date
                                                                     Signature
                                     183

-------
REVISIONS:

EVAPORATIVE EMISSIONS
PREPARATORY PROCEDURES
TEST PROCEDURE
PROCEDURE NO.
T-o-in-) —
PAGE-L-OF J. —
 9.0 DATA INPUT

     9.1  Fill in Sections I,  II,  III on form 701-01

     9.2  Turn form into Data Validation section for transfer of information
          onto CVS data sheet

10.0 DATA ANALYSIS

     10.1 Data entered into Section III must be analyzed to assure that
          they are within specified acceptable limits.

11.0 DATA OUTPUT

     11.1 Section III information  becomes part of the final certification
          results via CVS data form

     11.2 Form No.701-01 filed in  Data Validation Office.

12.0 ACCEPTANCE CRITERIA

     12.1 All items must be evaluated.   Tolerances:  CO  to  be ±.5% and
          RPM to be ±150 RPM

13.0 QUALITY PROVISIONS

     13.1 Institute corrective action if all required data is not filled in.

     13.2 Notify Certification Branch representative if out of "specification
          limits"
                                    TSF

-------
Vehicle mfgr.
 F.T.P. MINUS EVAP PLUS F.E.T.

DRIVER'S PRECONDITIONING REPORT


                      No.
Time Out Time In
Date
I. VEHICLE INSPECTION
A. Valid License Plate
B. Exhaust Adaptor
C. Fuel Drain
D. Vehicle Damage
Odom

Testft
DOK
DOK
DOK
DOK
D.None
DNone
D None
DNote
F.
G.
H.
I.
Mfgr's Data Sheet D OK
Oil level; if low dOK
notify Prod. Cont.
Odom Reading DOK
Fuel level, 1/4-
DNone
D Note

         (note on reverse)

    E.  Equip, not con-
        nected lotify
        Prod. Cont.
       D OK   D Note
   tank min,;  add if
   required.

J. Start-up per Mfg. DOK
   instructions

K. Drive AMA route   DOK
    AMA PRECONDITIONING

    A.  Engine Start

    B.  Ignition Switch

    C.  Starter Motor

    D.  Fast Idle

    E.  Transmission

    F.  Clutch

    G.  Brakes

    H.  Driveability
     DGood          D Hard

     DOK            D Other

     D OK            D Grinds

     D OK            D None

     D OK            D Shifts Hard

     D OK     Grabs  D Slips

     D OK     Fade   D Poor
               D False



               D No Start

               D Engine Hot



               D N/A

               D None
     D Surge  DStumble  DBack Fire  D Stretchy
       Engine Miss D       DieselsO
     D OK
    Driver's Signature
    Form 701-01
                                   185

-------
II.  SPECIFICATION CHECK                                       INITIAL
     A.  Idle CO             Rt
     B.  Engine RPM          Idle	    Drive_
     C.  Ignition Timing     	@	in DD/ND

     D.  Fuel Drain

     E.  Wheel to driveshaft ratio
         '10 wheel turns to 	driveshaft revs. N/V	

     F,  Tire size        x       .
     G.  Vehicle Weight 	with 	 tank fuel

     H.  Add 40% evap. fuel.  Witness Sig. 	
TV.  DYNAMOMETER HOT LA-4

     A.  Drive vehicle onto dyno.
         Set inertia 	Ibs. @	H.P.

     B.  Check Varian.  OPaper-OK  DPen-OK  DInk-OK  DZero-OK

     C.  Start Cooling Fan  DOK  DRelease Dyno Brake-OK
                            DTire  Pressure 45 P.S.I.-OK

     D.  Hook-up   DChock Blocks-OK   DCable Winch   DExhaust

     E.  Drive to Soak Area per schedule.

     F.  11-Hour Soak Start 	  (DO NOT RE-START ENGINE
         AFTER SHUT DOWN).

     G.  DO NOT START TEST BEFORE 	AM/PM.  (Add 11 hours
         to hot soak start time).
     Technician's Signature


     Leader/Supv. Signature
                                       186
        Form 701-01 Cont.

-------
                                    EPA PRE-CO:.DITIGi:iNG ROUTE
 60  sec  idle before leaving EPA
 EPA Lab.  East on PLYMOUTH RD.
 PLYMOUTH  RD. to GREEN P.O., right turn
 GREEII P.O.  to GLACIER, left turn
 GLACIER to EARHART. right turn
 EARHART to GECDES, left turn
 GEDDES  to  US-23N
 WOT accel.  to 55 r.ph on US-23;:, US-23:: to  PLYMOUTH  RD.,  right turn
 PLYMOUTH  RD. to DIXCCRO P.D., right turn
 DIXEORO RD.  to GECOES, right turn
 GECDES  to  jet. w/FULLER to '.:ALL ST., right turn
 Stop on WALL ST., idle for 2 minutes
 KALL ST.  to  EROAD'.:AY, left turn
 BROADWAY  to  jet.  u/EEAKES
 EEAKES  to  FIFTH ST., left turn
 FIFTH ST.  to KURO:;,  right turn
 l.llP.Ot; to FOURTH ST., right turn
 FOURTH  ST. to  CETPOIT ST., right turn
.DETROIT  ST.  to Dl'/iSIC:;,  left turn
 DIVISIC;; to  PLY: :ijTii r.a.
 PLYMOUTH P.O.  to US-23S'
WOT Bcccl.  to 55 r.ph  on  L'S-2
  Exit US-23S ot GiTDGES,  cr.t
li'OT cccnl.  to 55 i.vh  on  L'S-235,  LS-23S
  Exit 17 CAST, enter US-23N
HT f.ef.-l .  to 55 r;A  en  US-23N,  LS-23II
CCL'ill to ['..'C.'J Fi'"..y, right turn
I'jr.'/i rr./Y  to PLYVVJTI! F.a.. left turn
PLY::'. JT;: r.j. to EPA LA;J.
CO :,i:c irflt- at LAB.
                                                                                                                                                                                   s
                                                                                                                                                                                   g
                                                                                                                                                                                   2
                                                                                                                                                                                   >
                                                                                                                                  o
                                                                                                                                  ro

-------
 EPA   TEST   PROCEDURE
                                      Number
                             TP-703
                                                               Page
                                                        of
 SUBJECT
 "LA-4" VEHICLE PREPARATION
  Reference  FEDERAL REGISTER, VOL. 38, NO. 209,
 OCT. 31, 1973 - 85.075-12	
                                             Data Form No.
                                              701-01; SECTION IV
  Responsible Organization
 TEST OPERATIONS
                                             Computer Program
                                              NONE
  Test Witness /REVIEW
 MANUFACTURER'S REPRESENTATIVE, EPA CERTIFICATION ENGINEER
                                             Performance Interval
                                              PER CERT.VEHICLE
  Type of Test Report
 DATA SHEET
  Report Distribution QUALITY ASSURANCE, DATA VALIDATION,
 CERTIFICATION BRANCH, TEST DATA FILE
                                             Supersedes
                                            __ NEW	
                                             Superseded by
  REMARKS/COMMENTS
                            ORIGINAL RELEASE  APPROVALS
  Office
Program Mgmt
Lab.  Branch
Lab.Branch
  Section
Quality Assurance
Chief
Test Operations Chief
Signature
Date
                                     REVISIONS
 Change
 Letter
Description of Change
        Approval
Date
                                      189

-------
REVISIONS:


"LA-4" VEHICLE PREPARATION
TEST
PROCEDURE
PROCEDURE NO.
TP-703
pA^F 2 OF 4

1.0 PURPOSE

    To prepare certification vehicles for evaporative emission collection.

2.0 TEST ARTICLE DESCRIPTION

    2.1  Test vehicle prepared by manufacturer

3.0 REFERENCES

    3.1  Federal Register, Vol. 38, No. 209, Oct. 31, 1973 - 85.075-12

    3.2  EPA TRAINING MANUAL, "Light Duty Certification Testing Procedures"

4.0 REQUIRED EQUIPMENT

    4.1  Chassis dynamometer

    4.2  Drivers aid, Varian

    4.3  Cooling fan

5.0 PRECAUTIONS

    5.1  Assure vehicle is tied down with winch cable

    5.2  Inflate tires to 45 psi

    5.3  Insure room temperature is within 68  to 86 F.

6.0 VISUAL INSPECTION

    6.1  Check for proper set-up of test equipment.

7.0 TEST ARTICLE PREPARATION

    7.1  Add evaporative test fuel to 20% of tank capacity
         NOTE:  Technician and witness must sign the "Fuel Log" located in
         fueling area.

    7.2  Drive vehicle onto the dynamometer.  Shut off engine.

    7.3  Install chocks at front wheels and tie down with winch cable.
         Release Dyno brake first or the cable will be too taught.

    7.4  Hook up exhaust vent system to vehicle.

    7.5  Place cooling fan in front of vehicle and turn fan on.
                                      191

-------
REVISIONS:
                          "LA-4" VEHICLE  PREPARATION
                          TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                      TP-703
  8.0 TEST PROCEDURES
  Test Sequence

      101


      102

      103


      104



      105


      106
            Test Description
Set inertia weight and hp per manufacturer's recom-
mendation.   Release dyno brake.

Calibrate driver's aid at 50 mph and zero.

Drive the hot  LA-4, following tolerances stated
in paragraph 85.075-14 of the Federal Register.

Upon completion of the LA-4 shut-off fan, engage
the dyno brake, remove exhaust vent  system, dis-
connect winch  cable and remove chocks.

Drive vehicle  to soak area, shut-off engine, record
the start time of the eleven hour soak.

Lock the vehicle and return the  keys to the
Production  Control office.
Data Output
Driver's
Chart
Date,  Time
                                      192

-------
REVISIONS:


"LA-4" VEHICLE PREPARATION
TP
-------
                        P.T.P. MINUS EVAP PLUS F.E.T.
                       DRIVER'S PRECONDITIONING REPORT
Vehicle
mfgr.

Time Out
Date
I.







No.

Time In

Testtf



Odom







VEHICLE INSPECTION
A.
B.
C.
D.
Valid License Plate
Exhaust Adaptor
Fuel Drain
Vehicle
Damage
D
D
D
D
OK
OK
OK
OK
D.None
D None
D None
DNote
F.
G.
H.
I.
Mfgr
's Data
Sheet DOK
Oil level; if low DOK
notify Prod. Cont.
Odom Reading DOK
Fuel
level/
1/4-
DNone
DNote

         (note on reverse)
     E.  Equip, not con-
         nected notify
         Prod. Cont.
     OK    O Note
   tank min,; add if
   required.
J. Start-up per Mfg. DOK
   instructions
K. Drive AMA route   DOK
II.   AMA PRECONDITIONING
     A.   Engine Start
     B.   Ignition Switch
     C.   Starter Motor
     D.   Fast Idle
     E.   Transmission
     F.   Clutch
     G.   Brakes
     H.   Driveability
 QGood           D Hard
 DOK             D Other
 D OK             D Grinds
 D OK             D None
 D OK             D Shifts Bar.
 D OK     Grabs   D Slips
D OK     Fade    D Poor
               D False

               O No Start
               D Engine Hot

               D N/A
               D' None
D Surge   DStumble   DBack Fire  D Stretchy
  Engine Miss D       DieselsD
D OK
    Driver's  Signature
     Form 701-01
                                   194

-------
                             Rt
                             Idle
II.   SPECIFICATION CHECK

     A.  Idle CO

     B.  Engine RPM

     C.  Ignition Timing

     D.  Fuel Drain
     E.   Wheel to driveshaft ratio
         10 wheel turns to
     F.   Tire size
                     x
                                                          INITIAL
                                      Lt
                                      Drive
                                             in DQ/ND
                                driveshaft revs. N/V
     G.  Vehicle Weight
                                  with
                                            tank fuel
H.  Add 40% evap.  fuel.  Witness Sig.
IV.   DYNAMOMETER HOT LA- 4

     A.   Drive vehicle onto dyno.
         Set inertia       Ibs.  @
                                       H.P.
B.  Check Varian.   QPaper-OK   D Pen-OK   D Ink-OK   D Zero-OK

C.  Start Cooling Fan   D OK  D Release Dyno Brake-OK
                        DTire   Pressure 45 P. S.I. -OK

D.  Hook-up    D Chock Blocks-OK   D Cable Winch    D Exhaust

E.  Drive to Soak Area  per schedule.
     F.   11-Hour Soak Start
         AFTER SHUT DOWN) .
     G.   DO NOT START TEST BEFORE
         to hot soak start time) .
                                            (DO NOT RE-START ENGINE
                                        AM/PM.  (Add 11 hours
Technician's Signature_
Leader/Supv. Signature
                                 195
   Form 701-01 Cont.

-------
EPA TEST
PROCEDURE HUmbr-7nd Paae , of ,
SUBJECT
TEST VEHICLE FUELING PROCEDURES
Reference
EPA MEMO DATED:
Data Form No.
9-5-74 704-01
Responsible Organization Computer Program
TEST OPERATION NONE
Test Witness/REViEW Performance Interval
PREP. TEAM LEADER PER. CERT. VEHICLE
Type of Test Report Supersedes
DATA c;HT?FT NEW
Report Distribution Superseded by
QUALITY ASSURANCE, TEST OPERATIONS, CERTIFICATION BRANCH
REMARKS/ COMMENTS
ORIGINAL RELEASE APPROVALS
Of f i ce
PROGRAM M(7MT
LAB . BRANCH
LAB . BRANCH



Change
Letter
Section Signature
nnAT.TTY A.QPTTRAN^E
CHIEF
TEST OPERATIONS... CHIEF


Date





REVISIONS
Description of Change Approval

Date i

197

-------
REVISIONS:


TEST VEHICLE FUELING
TCCT PPOfFniiPF
1 CO 1 r l\vx\* t Ix wl\C
PROCEDURE NO.
TP-704
PAriF_2,,.OF 5

1.0  PURPOSE

     This procedure is designed to assure that the correct fuel is put into each
     certification vehicle.

2.0  TEST ARTICLE DESCRIPTION

     Certification vehicle.

3.0  REFERENCES

     3.1  EPA MEMO, - "TEST VEHICLE FUELING PROCEDURES," 9-5-74.

     3.2  EPA, ANN ARBOR, DRAFT, "LIGHT DUTY TEST OPERATIONS."

4.0  REQUIRED EQUIPMENT

     4.1  Fuel Conditioning Carts and Related Equipment, (i.e., nozzles,  etc.)

     4.2  Fuel-Indolene HO clear (unleaded)  or Indolene 30 (leaded)

     4.3  Remote Control Door Openers.

5.0  PRECAUTIONS

     5.1  All safety precautions for vehicle fueling must be followed.

          o    No smoking
          o    Electrical equipment grounded
          o    Fuel carts grounded with ground cables
               (not to insulated bumpers)
          o    Vehicle being fueled must be grounded
          o    "Absorbent" material to cover fuel and oil spills

     5.2  Assure lead fuel is not used for catalyst equipped vehicles.

6.0  VISUAL INSPECTION

     6.1  Assure ground cables are properly connected.

     6.2  Check for proper color coding of fuel used for vehicles

          6.2.1     Indolene 30 "leaded" marked with green paint

          6.2.2     Indolene HO-clear "unleaded1  marked with red or  orange paint.
                                      199

-------
REVISIONS:

TEST VEHICLE FUELING
TEST
PROCEDURE
PROCEDURE NO.
TP-704
PAGE 3 OF 5 	
7.0  TEST ARTICLE PREPARATION

     7.1  All fuel nozzles,  data sheets,  vehicles,  and  fuel  carts  are  marked
          a color code relating  to  fuel requirement.

          o    Orange or red for Indolene HO  clear  (unleaded)
          o    Green for Indolene 30  (leaded)

     7.2  Before driving the "AMA"  cycle, the driver must obtain the appro-
          priate remote control  unit  from Production Control.  NOTE:   Remote
          controls have frequencies corresponding to the applicable fuel
          prep cell.
                                    200

-------
REVISIONS:
                          TEST VEHICLE FUELING
                           TEST    PROCEDURE
PROCEDURE NO.
   TP-704	
PAGE.i__OF .5	
  8.0  TEST PROCEDURE
       The test vehicle fueling procedures specified below must be followed in
       all instances  to assure proper fuel handling.
  Test Sequence              Test Description
     Data Output
       101      Production Control will stamp  the fuel require-        Color Code
                ments on all^work sheets and check lists assoc-
                iated with each vehicle.

       102      The  prep, technician will place appro-
                priate orange or green label next to the fuel
                filler door, steering wheel area and on the
                side window.

       103      Fuel nozzles in each of the two prep cells is
                appropriately color coded.  Assure the color
                matches that on the vehicle.

       104      Upon return from the "AMA" route enter the prep
                cell that opens when the remote control unit
                is activated.

       105      Before fueling any test vehicle, verify the
                type of fuel required and nozzle type.  The
                check sheet is to be signed by the technician
                and EPA witness.

       106      Following the  vehicle fueling the technician          Date, Vehi-
                and EPA witness shall log the date,  vehicle,           cle, Vehi-
                vehicle number, type of fuel, and number of           cle type,
                gallons pumped on the Vehicle Test Fuel               Fuel, Gals.
                Record," and sign it off.
                                     201

-------
REVISIONS:

TEST VEHICLE FUELING
TEST PROCEDURE
PROCEDURE NO.
TP-704
PAGF 5 OFJL-
9.0  DATA INPUT

     9.1  Sign off checksheet #705-01 (Section I)  and Section III of form #702-01.

     9.2  Fill out the "Vehicle Test Fuel Record," form #704-01.

10.0 DATA ANALYSIS

     None required

11.0 DATA OUTPUT

     11.1 Forms 702-01 and 705-01 stay with vehicle until all tests are complete.

12.0 ACCEPTANCE CRITERIA

     12.1 Assure the proper fuel has been dispensed for each vehicle.

     12.2 All forms must be completed and signed.

13.0 QUALITY CONTROL PROVISIONS

     13.1 Reject vehicle data if improper fueling  has occurred and contact
          supervisor and manufacturers representative for disposition  of
          the vehicle and appropriate corrective action to follow.

     13.2 Institute corrective action (drain improper fuel)  and repeat
          the procedure.
                                      202

-------
                                  VEHICLE  TEST FUEL RECORD

1









ro
o
OJ
















'REP. ROOM #


DATE





















1
1




VEHICLE






















I
FUEL TYPE: 1.
2.
3 .
]
VEHICLE NO.









-
















i
TYPE
FUEL





















I
r




GALS .






















1
PUMP RE AD INC



SIGNATURE OF TECH.





















\

I: 1.
2.
3.

SIGNATURE -WITNESS







i













I



























1

FORM 704-01

-------
                   VEHICLE TEST AND  EVAPORATIVE DATA



                                              No.
Inertia Wt . HP A/C
Test 0


I. HEAT .BUILD

A. Drain fuel

B. Plumb air cleaner

C. Plumb canister

D. Plumb bowl vent (if required)

E. Trap gas cap (if required)

F. Seal orifices/vents

G. Install carbon traps (record on

H. Hook-up temperature recorder

I. Hook-up thermocouple leads

J. Install heat blanket
'
K. Plug in fuel tank heater (when

TECH
D

n

D

D

D

D

Q
data sheet)
D

D

D

D
used)
D
CTA
D

n

D

a

a

a

n

a

a

a

a

a
L. Refuel vehicle - 40% of tank capacity
Tech. Sig.
M. Replace fuel cap, plug exhaust
Heat Build Fuel Temp. Fuel Temp.
Progress Lead No. 1 Lead No. 4
0-Min.
15-Min.
30-Min.
45-Min.
60-Min.
Witness Sig.
pipe(s) Unclamp canister Q
Ambient
Temp .






a








II. DYNAMOMETER WARM-UP/SET
A. Drive non-test vehicle onto dyno
C. Set inertia Ibs.Q II. P.
h. Remove vehicle from dvno
I. Tech. Sig.
II. Tech. Sig.


B. Hook-up vehicle as for Hot LA
D. Drive @50mph steady state
Date
Date


FORM 705-01

-------
       FORM 705-01  (Continued)


III.  MASS- EXHAUST EMISSIONS TEST

      A.   Check Varian   Papcr-OKD Pen-OKQ  Ink-OKQ  Zcro-OKD

      B.   Cooling fan in place   OKQ Release  dyno  brakc-OK Q

      C.   Hook up     Chock blocks-OKQ  Cable winch n   Exhaust Q

      D.   Temp, recorder   Connect thermocouple  leadsQ  Start  recorder

      E.   CVS    Check fan opcrationQ Bags-OK'D Rev.  Ctr.  Zero Q
                 Leak chcck-OK  C      CVS Temp-OK  Q
                 Cell tcmp-OK   G      Return  to  sample  Q

      F-   Drive test trace  [j     Check tire pressure  (45 PSI)   £J

      G.   Remove vehicle to Soak Area  f!
 IV.  HOT SOAK EVAPORATIVE EMISSION'S TEST                        TECH   CTA

      A.  Reseal orifices/vents                                   Q    Q

      B.  Reconnect carbon canisters and unclamp                  *-*    '-'

      C.  Reconnect temp, recorder and thermocouple leads         Q    Q

      D.
                                                                 D   D
     . E.   Plug exhaust pipe(s)                                   Q   Q

      F.   1-hour soak  Start time	 End	                r-,    ,-,

      G.   Start amb.  temp.	 End amp. temp.	            m    r-j

      H.   Check ambient temp, at 15-min. intervals               Q    Q

      I.   End of hot  soak - reclamp canisters and remove         D    D

      J.   Shut-off temp, recorder                                ,-,    _

      K.   Weigh canisters and record on data sheet              r~,    .-,

  V.   DE-PREP AND VEHICLE REMOVAL

      A.   'Remove all  collection tubing, exhaust pipe plug(s),
          orifice/vent plugs, tape, foil, etc.                  CD    D
      B.   Disconnect  temp, recorder f( thermocouple leads        Q    p
      C.   Return engine to Mfgr's running configuration         n    G
      D.   Move vehicle to East lot - keys to Prod. Contr.       Q    Q
      E.   "VOID" or "FAILED" vehicles - check with Team Leader
          for disposition
      F.   Leave as is, if acceptable for IIWFET
III.   Tech.  Sig.	 Date	
 IV.   Tech. Sig.
                         	Date
                                      205  '
V.  Tech. Sig.	Date

-------
  EPA    TEST    PROCEDURE
                                      Number
                           TP-705
                                                                Page       of
  SUBJECT
  DIURNAL EVAPORATIVE TEST  (HEAT BUILD)
  Reference      FEDERAL REGISTER, VOL. 38, NO. 209,
  Oct. 31. 1973. Section 85.075-13 - 85.075-21	
                                             Data Form No.
                                             705-01
  Responsible Organization

  TEST OPERATIONS
                                             Computer Program
  Test Witness/Review
  MANUFACTURER"S EPA REPRESENTATIVE
                                             Performance Interval
                                             As per each Cert.Veh
  Type of Test Report
  DATA SHEET
  Report Distribution
  CERTIFICATION BRANCH, DATA VALIDATION, QUALITY ASSURANCE
                                             Supersedes
                                             NEW	
                                             Superseded by
  REMARKS/COMMENTS
                            ORIGINAL RELEASE APPROVALS
  Office
   Section
Signature
Date
Program Mgmt
Quality Assurance
Lab Branch
Chief
Lab Branch
Test Operations Chief
                                     REVISIONS
 Change
 Letter
 Description of Change
        Approval
Date
                                      207

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REVISIONS:

DIURNAL EVAPORATIVE TEST (HEAT BUILD)
TEST
PROCEDURE
PROCEDURE NO.
TP-705
PAfiF 2 OF 6
1.0  PURPOSE

     To quantify evaporative emission losses occurring during a simulated
     diurnal temperature rise period.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Certification Test Vehicle.

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 209, Oct. 31, 1973 - Sec.  85.075-13,
          85.075-21

     3.2  EPA Training Manual, "Light Duty Certification Testing Procedures."

4.0  REQUIRED EQUIPMENT

     4.1  Drying tubes - 3/4 in. ID, tubular, transparent

     4.2  Desiccant, 8 mesh

     4.3  Collection tubing, stainless or aluminum,  5/16 ID.

     4.4  PVC tubing, 5/16 ID.

     4.5  Hosecock clamps, rubber plugs, aluminum foil,  tape

     4.6  Balance - accuracy ±.075 grams

     4.7  Temperature recorder, multi-channel, range 50   to 100 F,  accuracy  ±1 F

     4.8  Type "J" thermocouples, iron-constantine

     4.9  Carbon traps, activated carbon, 300 ±25 ml, capacity 150  gms  activated
          carbon

          4.9.1     Heat blanket

5.0  PRECAUTIONS

     5.1  Follow vehicle fueling safety precautions
                                                      o        o
     5.2  Soak temperature (ambient)  must be between 76  F and 86 F.

     5.3  Do not place canisters on floor or suspend from collection  tubing,
          DO NOT KINK LINES.  Place canister on a stand.
                                     209

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REVISIONS:

DIURNAL EVAPORATIVE TEST (HEAT BUILD)
TEST
PROCEDURE
PROCEDURE NO.
TP-705
PAGE 3 OF_L_
6.0  VISUAL INSPECTION

     6.1  Inspect all plumbing and electrical connections.

     6.2  Check color coding to insure proper evap.  fuel is used.

7.0  TEST ARTICLE PREPARATION

     7.1  Drain the fuel tank completely.

     7.2  Install collection tube on the air cleaner.

     7.3  Install collection tube on the vehicle carbon canister.

     7.4  Seal all other orifices and vents to the atmosphere including exhaust
          pipe(s) and heat stove orifice.

     7.5  Install collection tube on open bowl vent.

     7.6  Seal fuel cap area for carbon trap after fuel is  put in.

     7.7  Install the temperature recorder.

          7.7.1     Plug the thermocouple lead coming  from  the fuel tank into
                    Channel 1.

          7.7.2     Install a two foot thermocouple  lead under the  hood by taping
                    "J" type thermocouple to the air cleaner snorkel.   The con-
                    nector should hang outside of the  engine compartment on the
                    right side  of the vehicle.   Plug into Channel  4.

          7.7.3     Channel 2 of the temperature is  permanently designated as
                    the ambient room temperature hook-up.

          7.7.4     Insure that all applicable switches inside of  the  recorder
                    are turned  on.

     7.8  Install a heat-blanket on cars without one previously installed.  Use
          one  blanket on each tank if the vehicle has  dual  tanks.   NOTE;  DO NOT
          PLUG BLANKET IN UNTIL THE TEST IS BEGUN!
                                       210

-------
REVISIONS:
                       DIURNAL EVAPORATIVE TEST (HEAT BUILD)
                           TEST     PROCEDURE
                                                  PROCEDURE NO.
                                                      TP-705

                                                  PAGE_1_OF _§_
 8.0  TEST PROCEDURES

      The following steps are to be followed to assure proper heat build for
      the diurnal breathing loss test.  As each step is completed check off
      on data form 705-01.
 Test Sequence
      101
      102
      103
      104
          Test Description

Obtain carbon traps for  each point to be
sampled on the vehicle.

Record the test number,  date and vehicle make
on the evaporative emission data sheet #705-01.
Record the identification  number marked on
canisters and location on  form #705-01.  The
lowest number will be  placed on the air cleaner.
Weigh each canister to  the nearest 0.05 gram.
If a deviation of ±.5 gram from the manu-
facturer's weight is discovered mark canister
for return to manufacturer.
Data Output
Test number
Date,  Vehi-
cle make

Canister
number in
descending
order -
location
      105
Clamp, with hose-cock clamps, within 1 to
1-1/2 inches of the  in/out tubes of the canis-
ters.  Cut off hose  in excess of 4 inches.
      106      Weigh  the canisters with the hose-cock clamps  in
               the  closed position.  Mark the weight on the
               canisters and record on form #028-02 in the
               space  marked initial weight.

      107      Recirculate evap. fuel in the fuel conditioning
               cart to allow for temperature stabilization.

      108      Add  evap. fuel to the fuel tank,  40% of the
               fuel tank capacity.

      109      Turn on temperature recorder and  monitor
                                          Should be
                                                      Initial
                                                      weight,
                                                      grams
initial fuel temperature.
60°F ±2°F,  log  on  form #7(
start time,  temp,  of  lead #4 and ambient temp.
                60°F ±2°F, log on form #705-01 along with
Amount of
fuel added

Fuel temp-
Lead #1,
Lead #4
ambient in
o
 F start time
                                       211

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REVISIONS:
                       DIURNAL EVAPORATIVE TEST (HEAT BUILD)

                           TEST    PROCEDURE
                                                  PROCEDURE NO.
                                                      TP-705	

                                                  PAGE_5
 Test Sequence
      110
      111
      112
      113
      114
          Test Description

Replace the fuel cap,  plug the  exhaust pipe
and unclamp the canisters.

Attach hose from the top  (inlet) of the canis-
ters to the evaporative collection tubing on
the vehicle.  The hose from the side  (outlet)
of the canisters are attached to a desiccant
tube.  The open end of tubing from desiccant
shall be taped at the  approximate height of
the trapping point to  allow for pressure
equalization.

Start heat build;  at 15 min. intervals record
fuel temp, of (fuel tank),  lead 4 (under hood
and ambient temperatures  on evap. data sheet
#705-01.  NOTE;  Adjust variac  to approximate-
ly 40.

At the end of one hour, shut off the variac,
unplug and remove the  heat  blanket, clamp off
the canisters (inlet side  first) and
return air cleaner and vehicle  carbon
canister to "running"  configuration.

Re-route fuel to carburetor and reinstall
heat stove tube.  Unplug  tailpipe, temperature
recorder and remove.
Data Output
      115       Recheck to assure all orifices/vents  to  atmos-
                phere are unobstructed; air cleaner,  heat  stove
                functioning; thermocouples and heat blanket dis-
                connected; plugs removed from tailpipe(s).

      116       Push vehicle onto dynamometer for  '75 FTP
                Emission test.
Lead 1, Lead
4, ambient
                                      212

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REVISIONS:

DIURNAL EVAPORATIVE TEST (HEAT BUILD)
TFST
pporpniiPF
PROCEDURE NO.
TP-705
PA^F.,6 OF 6
9.0  DATA INPUT

     9.1  Fill in Test no., date, make of car, test no, canister numbers, location
          and initial wt. of canister on form #705-02  (Evaporative Emission
          Weighing Data).

     9.2  Fill out section I "Heat Build" of form #705-01  (Vehicle Test and
          Evaporative Data).

10.0 DATA ANALYSIS

     10.1 No analysis other than procedural verification is accomplished until
          the completion of the hot soak evap. test.

11.0 DATA OUTPUT

     11.1 Form 705-01 stays with the test vehicle until the completion of the
          Hot Soak Evaporative Test and submitted to Data Verification following
          De-prep and removal.

     11.2 Form 705-02 also remains with the test vehicle until the weight of the
          canister has been recorded for the Hot Soak Evap. Test.

12.0 ACCEPTANCE CRITERIA

     12.1 During the heat build the fuel in the tank is to be heated from 60°F ±2°F
          to 84 F ±2 F at a constant rate of change over a 1 hour ±10 minute period

     12.2 The ambient temperature of the soak area must remain within the 76°F
          to 86 F band.

     12.2 After a minimum of one hour in the soak area the vehicle must be moved
          (pushed) onto the dynamometer for the '75 FTP.

13.0 QUALITY PROVISIONS

     13.1 Form #705-01 has a built in quality check in Section I.  Each step per-
          formed is checked off by the technician and then checked and signed
          off by a witness, thus an audit is performed at the site of the test.

     13.2 Heat build progress should be audited by the Q.A. department to
          assure the specified limits have not be exceeded.

     13.3 All deviations (if any)  from the prescribed procedure should be
          documented fully on form 705-01.
                                      213

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                   VEHICLE TEST AND EVAPORATIVE DATA



                                              No.
Inertia Wt. HP A/C
Test $

I. HEAT -BUILD

A. Drain fuel
B. Plumb air cleaner

C. Plumb canister

D. Plumb bowl vent (if required)

E. Trap gas cap (if required)

F. Seal orifices/vents

G. Install carbon traps (record on

H. Hook-up temperature recorder

I. Hook-up thermocouple leads

J. Install heat blanket

K. Plug in fuel tank heater (when

TECH CTA
D D

D D
D D

D D

D D

D D

n n
data sheet) u u
D D

D D

D D

D D
used)
D D
L. Refuel vehicle - 401 of tank capacity
Tech. Sig.
M. Replace fuel cap, plug exhaust
Heat Build Fuel Temp. Fuel Temp.
Progress Lead No. 1 Lead No. 4
Witness Sig.
pipe(s) Unclamp canister £J Q
Ambient
Temp.
0-Min.
15-Min.
30-Min.
45-Min.
60-Min.

II. DYNAMOMETER WARM-UP/SET
A. Drive non-test vehicle onto dyno
C. Set inertia lbs.@ II. P.
h. Remove? vehicle from dvno
I. Tech. Sig.
II. Tech. Sig.
on I,

B. Hook-up vehicle as for Hot LA-4
D. Drive @50mph steady state
Date
Date
FORM 705-01

-------
       FORM 705-01 (Continued)


III.   MASS. EXHAUST EMISSIONS TEST

      A.   Check Varian   Paper-OKQ Pen-OKQ Ink-OKQ Zero-OKD

     ' B.   Cooling fan in place   OKQ Release dyno brake-OK Q

      C.   Hook up     Chock blocks-OK D  Cable winchn  Exhaust Q

      D.   Temp, recorder   Connect thermocouple leadsQ Start recorder Q

      E.   CVS    Check fan operationQ Bags-OKD Rev. Ctr. Zero  Q
                 Leak chcck-OK £      CVS Temp-OK n
                 Cell temp-OK  Q      Return to sample  Q

      F.   Drive test trace  £3     Check tire pressure (45 PSI)  Q

      G.   Remove vehicle to Soak Area  n

 IV.   HOT SOAK EVAPORATIVE EMISSIONS TEST                       TECH  CTA

      A.   Reseal orifices/vents                                  Q    Q

      B.   Reconnect carbon canisters and unclamp                 '-'   ^

      C.   Reconnect temp, recorder and thermocouple leads        D   D
u . unecK
gab cap

E. Plug exhaust pipe(s)
F. 1-hour
G. Start
H. Check
I. End of
soak Start time
amb . temp. End
End
amp. temp.
ambient temp, at 15-min. intervals
hot soak - reclamp
canisters and remove
J. Shut-off temp, recorder
K. Weigh
canisters and record
on data sheet
D
n
n
i-i j
n
n
n
D
n
D
D

n
n
D
n
n
  V.   DE-PREP AND VEHICLE REMOVAL

      A.  'Remove all collection tubing, exhaust pipe plug(s),
          orifice/vent plugs, tape, foil, etc.                  D    D
      B.   Disconnect temp, recorder § thermocouple leads        Q    [n
      C.   Return engine to Mfgr's running configuration         Q    n
      D.   Move vehicle to East lot - keys to Prod. Contr.       Q    Q
      E.   "VOID" or "FAILED" vehicles - check with Team Leader
          for disposition
      F.   Leave as is, if acceptable for IIWFET
III.   Tech.  Sig.	     	     Date	
 IV.   Tech. Sig,
                                                         Date
                                       215
  V.   Tech. Sig.	Date_

-------
            EVAPORATIVE  EMISSION WEIGHING DATA
     TEST NO.
     DATE
     MAKE OF CAR
CANISTER NO.
CANISTER LOCATION
HOT SOAK WEIGHT
INITIAL WEIGHT
EVAP. EMISSIONS





1 i














     TOTAL EVAP. EMISSIONS
FORM 705-02
                              216

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EPA TEST
Nui
PROCEDURE
nber
TP-706 page i of 9
SUBJECT
1975 URBAN DYNO TEST - FTP
Reference Federal Register, Vol.38, No. 209, Oct. 31, 1973 - Data Form No.
Sees. 85.075-14 thru 19 and 24, 25, Appendix I 705-01
Responsible Organization
Test Operations
Test Witness/Review
Manufacturers EPA Representative
Type of Test Report
Data Sheet
Computer Program
Analysis by SAQF:
NKwrvs
Performance Interval
Per Vehicle
Supersedes
New
Report Distribution Superseded by
Quality Assurance, Test Oper. ,Data Validation, Cert. Branch
REMARKS/ COMMENTS
1.0 See procedure No. TP-707 for sample
analysis of the 1975 FTP.
ORIGINAL RELEASE APPROVALS
Office
Pvorrr'^m MfTfp'h
Lab. Branch
Lab. Branch


Section
nii^ 1 i t-y AseiiTanr-fa
Chief
Test Operations Chief


Signature





Date





REVISIONS
Change
Letter
Description of Change
Approval

Date

217

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REVISIONS:

1975 Urban Dyno Test (FTP)
TEST PROCEDURE
PROCEDURE NO.
TP-706
? 9
DAftF Z ftF
1.0  PURPOSE

     To collect exhaust emissions utilizing a constant volume sampler.  The
     dilute exhaust emissions are collected in sample bags.   This sample
     is collected from a test vehicle which is being driven on a chassis
     dynamometer following the FTP driver's trace. The sample collected is
     then analyzed by the analysis system.
     (Ref.TP-707) .

2.0  TEST ARTICLE DESCRIPTION

     2.1  Manufacturer's certification vehicle.

3.0  REFERENCES

     3.1  Federal Register, Vol. 38, No. 209, Oct. 31, 1973, sections
          85.075-14 through 19 and 85.075-24 through 25 and APPENDIX I.

     3.2  EPA, Ann Arbor, Training Manual, "Light Duty Certification Testing
          Procedures."

4.0  REQUIRED EQUIPMENT

     4.1  Constant Volume Sampler equipped to meet requirements in Federal
          Register, Sec. 85.075-20.

     4.2  Chassis Dynamometer
               o    Clayton model ECE-50

     4.3  Drivers Aid
               o    Varian
               o    Hewlett-Packard

5.0  PRECAUTIONS

     5.1  Perform dyno warm-up procedure (TP-604)

     5.2  Ensure the hood of the test vehicle is closed and the cooling fan
          is turned off during the 10 minute soak.

6.0  VISUAL INSPECTION

     6.1  Insure fan and tail pipe connector are in place.

     6.2  Check bags for correct installation.
                                      219

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REVISIONS:

1975 Urban Dyno Test (FTP)
TEST PROCEDURE
PROCEDURE NO.
TP-706
PAGE.1-OF 2 —
7.0  TEST ARTICLE PREPARATION

     7.1  Insure test vehicle is aligned properly on the dynamometer and
          tied down.

     7.2  Inflate tires to 45 p.s.i.

     7.3  Daily Start-up (System Check-out);  check off in section III, form #705-01

     7.4  Check Varian for Paper,  Ink and calibrate zero; check off as above.

     7.5  Install sample bags

     7.6  When the cell technician/CVS operator  have confidence that the CVS and
          associated  equipment are operating  correctly,  the analyzer operator will
          have the manufacturer's  EPA representative check and approve vehicle
          for the test.
                                      220

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REVISIONS^
                          1975 URBAN DYNO TEST  (FTP)
                           TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                    TP-706
                                                 PAGE.
.OFj.
  8.0  TEST PROCEDURE

      The Mass Emission test data is  collected as a result of the
      dural steps.

  Test Sequence            Test Description

      101       Push test vehicle on  the dyno.

                     o    Release the dyno. brake.

                     o    Secure vehicle with the down cable(s).

                     o    Place chocks on front wheels

                     o    Install cooling fan 12 inches in front
                          of vehicle  and raise hood.

                     o    Install flexible exhaust hose.

                     o    Connect thermocouple leads to tempera-
                          ture recorder and turn on.
      102
      103
      104
      105
                                                 following proce-


                                                     Data Output



                                                     Dyno. brk. of:

                                                     Cable winch

                                                     Chocks

                                                     Cooling fan


                                                     Exhaust

                                                     Thermocouples
                                                     Start recorder
     o    Check form  #705-01, section III.

The CVS operator will:

     o    Zero counters

     o    Turn on "dia. pumps" and "blower."

     o    Inspect and install sample bags.

     o    Check CVS temperature.

     o    Check cell  temperature.

Prior to entering the vehicle the driver will:

     o    Assure fuel is properly connected.

     o    Become familiar with the manufacturer's
          starting procedure.

The driver will:

     o    Enter vehicle.

     o    Zero "drivers aid" and lower the  pen.

The operator will engage bags "1 and 3."


                      221
                                                                     Rev.  Ctr.  Zerc



                                                                     Bags

                                                                     CVS temp.

                                                                     Cell temp.

-------
REVISIONS:
                          1975  URBAN DYNO TEST  (FTP)

                           TEST    PROCEDURE
PROCEDURE  NO.
	TP-706

PAGE-L-OF J—
 Test Sequence                 Test Description

      106a      Proceed with manufacturer's starting procedures:

                     o    Simultaneously start "counter"
                          and  crank engine.

                     o    If engine starts and continues to
                          run,  turn on the driver's aid.

      106b      If vehicle cranks for more than 10 seconds,
                take the following steps:

                     o    Cease cranking

                     o    Shut off "rev counter"

                     o    Shut off CVS

                     o    Manufacturer's representative has 30  min.
                          to correct cause.

                     o    Repeat starting procedures in 106a.

      106c      If vehicle "false starts", repeat step 106a.

                     o    If unable to restart vehicle before first
                          accel, shut off varian until engine starts.

                     o    If vehicle fails to start in 10 seconds,
                          repeat step 106b.

                     o    If vehicle "false starts" repeatedly  for
                          60 seconds, the test is voided.

      107       If vehicle starts and runs properly, but stalls
                when shifted into gear at 15-second point,  shut off
                varian and re-start vehicle, shift back into gear,
                re-start varian and continue test.

      108       When engine  is  started, the driver  may use any  means
                necessary to keep engine running, i.e., "feathering"
                accelerator, "slipping" clutch, etc.
     Data Output
     Long crank
     False start
    Void

-------
REVISIONS:
                         1975 URBAN DYNO TEST (FTP)
                           TEST    PROCEDURE
PROCEDURE NO.
   TP-706
PAGE±	OF
 Test Sequence                Test Description                       Data Output

      109       The driver will follow the Federal  driver's trace,
                (see attachment A) with close attention given to
                the following:

                    o    Follow trace as closely as possible to
                         avoid "out of spec" conditions,  (see
                         attachment B for operating mode
                         instructions)

                    o    Monitor "trace" paper to  assure  it does not
                         get hung up.

                    o    In case of problems,  blow horn for
                         CVS operator.

      110       At the  "505 second point" the driver will  initiate
                sampling of "bags 2 and 4" for the  "stabilized" phase
                of the  test.

      Ill       At 1367 seconds the final idle begins.

                    o    At 1369 sec. the ignition will be
                         turned off.

                    o    Five seconds after the engine stops turning,
                         shut off the sample and counter.

                    o    Read rev. counts.                            rev.  counts

      112       After "rev. counter" has been turned off,  the
                10 min. soak begins.  The driver will:

                    o    Close the vehicle hood.

                    o    Shut off cooling fan.

                    o    Disconnect and shut off the CVS

                    o    If fuel vents are being trapped, trap is
                         removed during 10 min.  soak and  second 505.
                         To be reconnected at beginning of hot soak.

      113       9 Min.  into the 10 min. soak, the driver will:

                    o    Open hood.

                    o    Turn on fan.
                                      223

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REVISIONS:
                        1975 URBAN DYNO TEST (FTP)
                          TEST    PROCEDURE
                                  PROCEDURE NO.
                                     TP-706

                                  PAGE_LOF _9_
 Test Sequence
Test Description
Data Output
      114       The CVS operator will:

                    o    Install and evacuate  "bags 1 and 2."

                    o    Zero counter.

                    o    Turn on dia. pumps  and blower.

      115       The driver will perform the following:

                    o    Roll "drivers chart"  to the beginning
                         of next test.

                    o    Start the "505 Hot" portion of test.

                         NOTE:  Must be started between 10 and
                         and 11 mins. of soak.

      116       At the end of "505" the CVS operator will turn  off
               "rev counter."

      117       Remove tie-downs, exhaust connector, cooling fan,
               put hood down, dyno roll brake  up and drive the
               vehicle off dyno into the soak  area at minimum
               throttle.
                                     22k

-------
REVISIONS:

1975 URBAN DYNO TEST (FTP)
TEST PROCEDURE
PROCEDURE NO.
TP-706
PAGF 8 OF 9
9.0  DATA INPUT

     9.1  Fill out section III of form 705-01 as the  required  steps  are
          performed and sign form.

     9.2  Driver should sign and date the FTP "drivers  trace."

10.0 DATA ANALYSIS

     10.1 Drivers trace should be checked for "out of spec"  conditions.

11.0 DATA OUTPUT

     11.1 Form #705-01 is kept with vehicle until De-prep  and  removal  has  been
          accomplished.

     11.2 Drivers trace is submitted to Data validation and  becomes  part of
          vehicle file.

12.0 ACCEPTANCE CRITERIA

     12.1 Drivers trace generated from the FTP must be  within  the  following
          limits.  (See Figure 12-1.)
        o
        IU
             2 MPH
                         ALLOWABLE
                           RANGE
                        •1 Sec.

                        •— 1 Sec.
» * /
2 MPH /.
/i
'>
•»
, AUOW&Bl
^ RANGE
-1 Sec. 1
•*— 1 Sec.
                     t

                   TIME
TIME
            Fig. 12-1.  ALLOWABLE LIMITS FOR FTP DRIVERS TRACE

          12.1.1    The upper limit is 2 mph higher  than the  highest point  being
                    driven on the trace within  1 second of given  time.

          12.1.2    The lower limit is 2 mph lower than the lowest point  being
                    driven on the trace within  1 second of given  time.

          12.1.3    Speed variations greater than the  tolerances  described  above
                    (i.e., manual transmission  shifting) are  acceptable if  they
                    occur for less than 2 seconds on any  occurrence.

          12.1.4    Exceeding lower tolerance  (12.1.2) is acceptable
                    when restarting a stalled engine or if the  vehi-
                    cle is operated at W.O.T.  (wide  open throttle)
                                       225

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REVISIONS:

1975 URBAN DYNO TEST (FTP)
TEST PROCEDURE
PROCEDURE NO.
TP-706
PAGE 9 OF J_
13.0 QUALITY PROVISIONS

     13.1 The Quality Assurance section should inspect the drivers trace to
          assure the acceptable limits stated in section 12 have been
          followed.

     13.2 if "out of limits"  conditions are discovered,  Quality Assurance
          should request corrective  action.  (i.e.,  have Production Control
          reschedule vehicle  for test.)
                                     226

-------
                     VEHICLE TEST AND EVAPORATIVE DATA



Vehicle Mfgr.	No.
Inertia Wt . HP A/C

I.





















HEAT -BUILD
A. Drain fuel
B. Plumb air cleaner

C. Plumb canister

D. Plumb bowl vent (if required)

E. Trap gas cap (if required)

F. Seal orifices/vents
G. Install carbon traps (record on

H. Hook-up temperature recorder

I. Hook-up thermocouple leads

J. Install heat blanket
*
K. Plug in fuel tank heater (when

Test #

TECH
a
a
a

n

D

a

data sheet)
D

D

D

D
used)
D


CTA
D
D
D

n

D

n

n
D

n

n

n

n
L. Refuel vehicle - 40% of tank capacity










II.



I.
II.
Tech. Sig.
M. Replace fuel cap, plug exhaust
Heat Build Fuel Temp. Fuel Temp.
Progress Lead No. 1 Lead No. 4
0-Min.
15-Min.
30-Min.
45-Min.
60-Min.

DYNAMOMETER WARM-UP/SET
A. Drive non-test vehicle onto dyno
C. Set inertia Ibs.Q II. P.
H. Remove vehicle from dyno
Tech. Sig.
Tech. Sig.
Witness Sig.
pipe(s) Unclamp canister £J
Ambient
Temp.







B. Hook-up vehicle as for

D









Hot LA-
D. Drive (DSOmph steady state

Date
Date



  form 705-01                        227

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                                                                  form 705-01 (Cont)


III.   MASS- EXHAUST EMISSION'S TEST

      A.   Check Varian   Paper-OK'P Pen-OKQ Ink-O'KP  Zero-OKD

      B.   Cooling fan in place   OKQ Release dyno brake-OK  CJ

      C.   Hook up     Chock blocks-OK P  Cable winchp  Exhaust P

      D.   Temp, recorder   Connect thermocouple leadsp Start  recorder p

      E.   CVS    Check fan operationp Bags-OKP Rev.  Ctr. Zero p
                 Leak check-OK \~      CVS Temp-OK p
                 Cell temp-OK  [j      Return to sample  p

      F.   Drive test trace  p     Check tire pressure  (45 PSI)   Q

      G.   Remove vehicle to Soak Area  P

 IV.   HOT SOAK EVAPORATIVE EMISSIONS TEST                        TECH   CTA

      A.   Reseal orifices/vents                                   P    .p

      B.   Reconnect carbon canisters and unclamp                  u    ^

      C.   Reconnect temp,  recorder and thermocouple leads         P    P

      D.   Check gas cap                                           r-,    r-,

      E.   Plug exhaust pipe(s)                                    P     P

      F.   1-hour soak  Start time	 End	                p    ,-]

      G.   Start amb. temp.	 End amp.  temp.	            Q    r-j

      H.   Check ambient temp,  at 15-min.  intervals               p    p

      I.   End of hot soak  - reclamp canisters and remove         P    p

      J.   Shut-off temp,  recorder                                ._.

      K.   Weigh canisters  and record on data sheet              .-,   .-.

  V.   DE-PREP AND VEHICLE  REMOVAL
A. Remove all collection tubing, exhaust pipe plug(s),
orifice/vent plugs, tape, foil, etc.
B. Disconnect temp, recorder § thermocouple leads
C. Return engine to Mfgr's running configuration
D. Move vehicle to East lot - keys to Prod. Contr.
E. "VOID" or "FAILED" vehicles - check with Team Leader
for disposition
F. Leave as is, if acceptable for I1WFET
III. Tech. Sig. Date
IV. Tech. Sic. Date
228
V. Tech. Sic. Date
D
P
P
P


P
n
D
P



-------
                                       TP-706
                 ATTACHMENT A  FED. DRIVING CYCLE
120-
 g-PLACE TRANSMISSION IN GEAR
 u
  >i-START OF DRIVING SCHEDULE
            (CHART SPEED-FOUR INCHES PER MINUTE)
          FEDERAL DRIVING SCHEDULE
                    FEDERAL REGISTER
           Revised Volume 36  Number 55 • March 20, 1971
                     229

-------
                                                                 TP-706
                ATTACHMENT B - DRIVER'S OPERATING INSTRUCTIONS
                                 FOR 1975 FTP
1.   ALL OPERATING MODES

     a.  AUTOMATIC TRANSMISSIONS must always be in DRIVE position, except
         during first idle and when restarting engines.

     b.  BRAKES and ACCELERATOR must NOT be used simultaneously.

     c.  STEERING WHEEL must NOT be turned during a test.

     d.  MINIMUM THROTTLING must be used during all modes to maintain speed
         indicated on driving trace.

2.   IDLES

     a.  MANUAL TRANSMISSIONS must always be in gear with clutch  disengaged
         during all idles, except the first.

     b.  THROTTLING is NOT PERMITTED during any idle mode,  except the first,
         to prevent stalling.

3.   ACCELERATIONS

     a.  ALL accelerations must be made SMOOTHLY without using brakes.

     b.  If the vehicle cannot accelerate at the specified rates, accelerate
         at WIDE OPEN THROTTLE (WOT) until vehicle reaches speed  required at
         that time during the driving trace.  WOT must be noted on driving
         trace where it occurs.

     c.  Vehicles equipped with FREE-WHEELING or OVERDRIVE UNITS  shall  be
         tested with the unit locked out of operation.

     d.  AUTOMATIC STICK SHIFT transmission may be shifted as manual trans-
         missions at the requestor's option for development testing only.

4.   DECELERATIONS

     a.  ALL decelerations must be made SMOOTHLY using brake or accelerator
         to maintain required speed.

     b.  ALL decelerations must be made WITHOUT DOWNSHIFTING MANUAL TRANS-
         MISSIONS unless indicated on the driving trace.
                                     230

-------
                                                                   TP-706
                            ATTACHMENT B (continued)

     c.  DISENGAGE CLUTCH on manual transmissions when:

         (1)   Speed drops below 15 MPH.
         (2)   Engine ROUGHNESS is evident.
         (3)   Engine STALL is imminent.
5.   SHIFTING
     a.  MANUAL transmissions must be quickly shifted during acceleration from:

         (1)   1st to 2nd at 15 MPH.
         (2)   2nd to 3rd at 25 MPH.
         (3)   3rd to 4th at 40 MPH for 4-speed and 5-speed transmissions.
         (4)   4th to 5th at requestor's option for 5-speed transmissions.

     b.  When shifting MANUAL transmission the ACCELERATOR PEDAL must be
         released as the CLUTCH is disengaged and the PEDAL depressed as
         necessary to maintain a smooth transition when CLUTCH is re-engaged.

     c.  If the FIRST GEAR RATIO exceeds 5:1 on a 4 OR 5 SPEED MANUAL
         TRANSMISSION, eliminate use of first gear and quickly shift during
         accelerations from:

         (1)   2nd to 3rd at 15 MPH.
         (2)   3rd to 4th at 25 MPH.
         (3)   4th to 5th at 40 MPH for 5-speed transmissions.

         NOTE:  Requestor will specify first gear ratio if it exceeds 5:1.

     d.  DOWNSHIFT manual transmissions at the beginning of or during a power
         mode if the engine is obviously lugging.  NOTE:  "Lugging" on trace
         if downshift is required.
                                       231

-------
  EPA    TEST   PROCEDURE
                                      Number
                                              TP-707
                                                               page    1   of  7
  SUBJECT
           SAMPLE ANALYSIS OF  1975  URBAN DYNO TEST
 Reference    Federal Register, Vol. 38, No. 29, Oct.31,1973
Sec. 85.075-15 & 85.075-20	
                                                              -Data Form No.
  Responsible  Organization
Test Operations
                                                               Computer Program
                                                               SAQF:NEWCVS
  Test Witness/Review
Manufacturer's EPA Representative,  Data Validation
  Type of Test  Report
Computer Print-Out

  Report  Distribution  Manufacturer/Certification Branch/
Data Validation/Quality Assurance	
                                                               Performance Interval
                                                               Per Vehicle	   _
                                                               Supersedes
                                                               New
                                                               Superseded by
  REMARKS/ COMMENTS
  Office
Program
Lab. Branch
Lab. Branch
                            ORIGINAL RELEASE APPROVALS
                    Section
                  Qnality
                  Chief
                  Test OperatiQns_.£hj..ef_
Signature
Date
 Change
 Letter
                                     REVISIONS
                  Description of Change
        Approval
Date
                                      233

-------
REVISIONS:


SAMPLE ANALYSIS OF 1975 URBAN DYNO TEST
TEST PROCEDURE
PROCEDURE NO.
TP-707
PAfiF 2 OF 7

1.0  PURPOSE

     To measure the bag concentrations collected by a constant volume sampler.
     This exhaust sample is diluted to a constant volume and collected
     in sample bags.  The collected sample is then analyzed for hydrocarbons,
     carbon monoxide, carbon dioxide and oxides of nitrogen by a gas analysis
     system.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Manufacturer's Certification vehicle.

3.0  REFERENCES

     3.1  Federal Register. Vol. 38, No. 209, Oct. 31,  1973, sec.  85.075-15  and
          85.075-20.

     3.2  EPA, Ann Arbor, Training Manual "Light Duty Certification Testing
          Procedures."

     3.3  EPA, Ann Arbor, "Light Duty Test Operations," Draft.

4.0  REQUIRED EQUIPMENT

     4.1  Constant Volume Sampler.

     4.2  Mass Analytical System capable of measuring the following:

          4.2.1  Hydrocarbons - Flame lonization

          4.2.2  Carbon Monoxide - Infra-red (NDIR)

          4.2.3  Carbon Dioxide - Infra-red  (NDIR)

          4.2.4  Oxides of Nitrogen - Chemiluminescence

     4.3  "Working" gas mixtures analyzed using EPA Primary Standards.

     4.4  "Zero Gas", nitrogen or air, and fuel cylinder for FID.

5.0  PRECAUTIONS

     5.1  Safety precautions should be followed when handling compressed gases.
          NO and CO are toxic gases!

     5.2  Insure cylinders have adequate pressure for testing.
                                      235

-------
REVISIONS:

SAMPLE ANALYSIS OF 1975 URBAN DYNO TEST
TEST PROCEDURE
PROCEDURE NO.
TP-707
PAr.F 3 OF Z_
     5.3  Do not exceed maximum allowable time of 20 minutes .after  end of
          test when analyzing bag.

6.0  VISUAL INSPECTION

     6.1  Check flow rates and pressures.

     6.2  During the FTP and during analysis mode monitor all instruments,
          gauges, and recorders to assure no "out of spec" conditions exist.

7.0  TEST ARTICLE PREPARATION

     7.1  Perform daily start-up on analyzer train.

     7.2  Activate strip chart recorders and check zero/span.

     7.3  Install sample bags and insure no leaks are present.

     7.4  Change filter (sample)  before FTP begins .

     7.5  Start ambient temperature recorder.
                                      236

-------
REVISIONS:
                    SAMPLE ANALYSIS OF 1975  URBAN DYNO TEST
                           TEST     PROCEDURE
                                                 PROCEDURE NO.
                                                     TP-707
                                                 PAGE_1_OF 2.
 8.0  TEST PROCEDURE

      The 1975 Mass Emission Test results  are  calculated as a result of data
      collected from the following procedural  steps.
 Test Sequence
      101
      102
      103
      104
      105
      106
      107

      108
      109
          Test Description

Prior to starting the first  "505" of the FTP
the analyzer operator will calibrate the
analyzers and generate span  points on the
chart recorders.

After the driver  has switched to bags 2 and 4
upon completion of the "505" the Analyzer operator
will deliver "bags 1 and  3"  to the analysis
transfer system.

The analyzer operator will first analyze the
"background" sample (bag  I)  and log the numerical
range and value from chart traces of HC, CO, CO
NO  on form 707-02.
  x
Step 103 is repeated for  the  "sample" bag. (bag 3)
Counts, mileage and seconds  are recorded
for first set of bags on  form 707-01, CVS
Data sheet.

At the 660 point on the driver's trace for the
odd numbered dyno,  and 1020  sec. point for even
number dyno the CVS operator will record the
inlet and outlet pressure of the positive dis-
placement pump on the CVS data sheet.

Recalibrate as shown in step 101.

Upon completion of  the transient phase of the
FTP repeat steps 103 and  104 for "bags 2 and 4."
Record on form 707-02.
Record counts,  mileage and  seconds for
second set of bags on CVS data sheet.
Data Output
  Bkgd.
HC, Defl.
CO, Defl.
CO , Defl.
NO , Defl.

Deflections,
HC, CO,  CO
NO  - Sample
  x

Revs, sees.,
mileage
Inlet pressure
out. pressure
in inches of
Deflections,
HC, CO , and
NO .  BKGD.
ana sample.

Revs., sees.,
mileage
                                       237

-------
REVISIONS:
                       SAMPLE ANALYSIS OF 1975 URBAN DYNO TEST
                           TEST    PROCEDURE
                                    PROCEDURE NO.
                                          TP-707

                                    PAGE-L-OF 2—
Test Sequence
Test Description
Data Output
     110       Recalibrate as shown in step 101 for final "505."

     Ill       Upon completion of  "505" hot, repeat steps 103
              and 104 for "bags 1 and 3."
     112       Record rev.  counts, mileage and seconds for
              the third set of  bags.

     113       Perform a post calibration and record on chart.

     114       Record the average wet and dry bulb temperatures,
              heat exchanger temperature and barometric pressure
              on CVS data sheet (707-01).
     115       Record CVS hours, Horsepower and analyzer  train
              number.
     116       Prepare for next test.
                                       Deflections,
                                       HC, CO, CO2
                                       NOX.  Bkgd.
                                       and sample.

                                       Revs., sees.,
                                       mileage
                                      Wn, °F
                                      Baro. Pressure
                                      Baro. Hg

                                      Hours , CVS
                                      Hp-indicated
                                      train number.
                                      238

-------
REVISIONS:

SAMPLE ANALYSIS OF 1975 URBAN DYNO TEST
TEST PROCEDURE
PROCEDURE NO.
TP-707
PAttF 6 r>F 7
9.0  DATA INPUT

     9.1  Check form 707-01 (CVS data sheet) and assure that all required data
          has been filled in.

     9.2  Assure that numerical deflections of HC, CO, CO  and NO  have been re-
          corded on form 707-02 (Analyzer read-out) for each of tfte three phases
          of the FTP.

     9.3  The Certification Branch representative and the Manufacturer's repre-
          sentative will inspect the CVS data sheet, driver's trace and
          CVS temp, trace.  They will then sign CVS data sheet as valid or invalid.

     9.4  Data Validation will complete form 707-01 and submit to Data Branch.

10.0 DATA ANALYSIS

     10.1 Data analysis is performed by the SAQF:NEWCVS program.

     10.2 Analysis is performed on Drivers Trace as stated in section 12 of
          procedure #TP-706.

     10.3 Analysis of all other supporting data is performed by Data Validation.

11.0 DATA OUTPUT

     11.1 Following completion of the hot soak evap. all of the following informa-
          tion is entered into the vehicle test file.

          o    CVS Data sheet form #707-01

          o    Diurnal temp, trace

          o    Analyzer trace

          o    Drivers trace

          o    CVS temp, trace

          o    702-01, DRIVER'S PRECONDITIONING REPORT

          o    705-01, VEHICLE TEST AND EVAPORATIVE DATA

     11.2 Final copies of CVS  data sheet and composite gram per mile results will
          go to the Certification Branch and the Manufacturer's representative.
                                       239

-------
REVISIONS:

SAMPLE ANALYSIS 1975 URBAN DYNO TEST
TEST PROCEDURE
PROCEDURE NO.
TP-707
PAGF 7 OF ,7,
12.0 ACCEPTANCE CRITERIA

     12.1 Driver's trace must be within limits stated in section 12.0 of
          procedure #TP-706.

     12.2 CVS temperature trace must be within +10 F of set point for the entire
          test.

     12.3 Manufacturer's representative must accept preliminary results as valid.

     12.4 Analyzer post calibration must be within ±2 divisions of the initial
          span point.

13.0 QUALITY PROVISIONS

     13.1 Check tests results on an "audit" basis to assure acceptance criteria
          has been met.

     13.2 Initiate corrective action if "out of spec" conditions are discovered.
          (i.e., Production Control will reschedule vehicle)

-------
                                      CONSTANT VOLUME SAMPLER (CVS) DATA SHEET
"3
2 MANF.
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-------
        CODE  EQUIVALENCE

        CARD  1

        MANF  CODE  (COLS  1-3)

        010   AMERICAN MOTORS
        021   (CHKYS) CHRYSLER
        022   (CHRYS) DODGE
        023   (CHRYS) PLYMOUTH
        031   (FO NO CO) FORD
        032   (FO MO CO) LINCOLN
        033   (FO MO CO) MERCURY
        041   (CM) BUICK
        042   (CM) CADILLAC
        043   (Cll) CHEVKOI.ET
        044   (CM) OLDSMOBILE
        045   (01) PONTIAC
        046   (CM) CMC
        047   (CM) DETROIT DIESEL
        050   ABARTH
        060   A C CARS
        064   AICHI
        070   ASTON MARTIN
        080   AUTO CAR
        085   AUTO SI'ORT
        090   ALFA ROMEO
        095   AM GENERAL
        100   AVAUTI
        105   AUBURN
        110   AUSTIN MORRIS (BLMC)
        120   BMW
        125   BOLWELL
        130   BRISTOL
        135   BRICKLIN
        140   CHECKER
        150   CITROEN
        160   COMKER
        170   SAMCO (CORD)
        175   DACIA (ARO)
        180   DAT
        190   DAIHATSU
        200   MERCEDES BENZ
        205   DE TOMASO
        210   DUAL GIIAI
        215   DYHA TRUCK
        220   FfRRARI
        230   FIAT
        240   FORD OF ENGLAND
        245   FORD Or CCRMAVY
        250   HINO
        255   HAKLEY-DAVIDSON
        260   HONDA
        270   IIIC
        280   ISO
        290   ISUZU
        300   JAGUAR (BLMC)
        310   JENSEN
        320   JOHN FITCH
        330   JEEP (KAISER)
        340   LANCIA
        350   LOTUS
       360   MASERATI
       365   MOHS
        370   MORGAN
       380   NISSAN
       390   NSU
       400   OPEl.
       405   PANTHER
       410   PEUGEOT
       420   PORSCHE
       430   RENAULT
       440   ROLLS-ROYCE
       450   ROOTES
       460   ROVF.R  (BLMC)
       470   SAAB
       480   SHELBY
       490   MITSUBISHI
       495   SIA1RA
       500   SIMCA
       510   SKODA
       520   SS AUTOMOBILE
       530   TRIUMPH (BLMC)
       535   STUTZ
       540   SUZUKI
       550   TORINO
       560   TOYO KOCYO
       570   TOYOTA
       580   VAUXHALL
       590   VOLKSWAGEN
       600   VOLVO
       605   WHITE
       610   YENKO
       615   YAMAHA
       620   TVR
       630   SUSPENSIONS INT (OMEGA)
       640   AUDI
       650   MURKNA MOTORS
       660   FUJI HEAVY  1ND
 CODE  EQUIVALENCE

 670   HOSTEVERDI
 680   1KTER.MECCANICA (ITALIA)
 690   LAMBORCIUNI
 700   MARCOS
 710   ARMY
 720   WINNEBACO
 725   ALLIS CHALMERS
 730   CATERPILLAR
 740   CUMMINS
 750   HERCULES
 760   MACK
 770   PLRKINS
 180   SCANIA-VABIS
 790   CLASSIC
 800   TELEDYNE CONTINENTAL
 BIO   CASE
 820   DIAMOND REO
 830   HIGHWAY PRODUCTS,INC
 999   EXPERIMENTAL

 AIR CONDITIONING (COl 61)

   1   WITH
   2   WITHOUT

 DTILITY  VEHICLE  (COL 62)

   1   YES
   2   NO

 TRANSMISSION  (COL 63)

   1   AUTO
   2   3-SPEED
   3   4-SPF.ED
   4   5-SPEED
   5   SEMI-AUTOMATIC

 SHIFT  PATTERN (COL 64)

   1   STANDARD
   2   OPTIONAL

 TEST TYPE  (COLS  69-70)
                                                                                         CODE  F.QUIVALENCE
 00   VOID
 01   CERT  (F.MISSION DATA)
 02   CERT  (DURABILITY)
 03   CERT  (CORRELATION)
 04   SURVE1LIANCE
 05   EXPERIMENTAL
 06   FICLD SURVEILLANCE
 07   PARTICIPATES
 08   OTHER
 09   CVS CORRELATION
 10   RESEARCH
 11   CORRELATION (LAB)
 12   CERT  (RUNNING CHANCE)

TRAIN (COLS 74-75)
 1-97 AECAS
 98   PARTICULATES
 99   PROP SAMPLER

CARD 2
DRIVING CYCLE (COL 67)
      7-MODE
      LA-4
      LA-4 S3
      ANN ARBOR
      LA-4 S4
      9X7 MODE
      STEADY STATE
      OTHER
SOURCE CODE (COLS 69-70)

 01
 02
 03
 04
 05
 06
 07
 08
 09
 10
 11
 12
 13
 14
 15
 16
 17
MANUFACTURER
HERTZ DETROIT
HERTZ L.A.
AVIS
AIRWAYS CORP L.A.
ALPH CORP L.A.
CSA L.A.
PO OEPT DETROIT .
PO DEPT L.A.
L.A. COUNTY VEH
STATE OF CALIFORNIA
BORROWED FROM CORPS
AMHIICAN RACEWAYS. INC
DEALER USED CARS
EPA
GSA
MILITARY
                                     18   PRIVATE OWNER
                                     19   OTHER

                                    CARD 3

                                    FUEL INJECTION  (COL  13)
                                      1   YES
                                      2   NO
                                    FUEL SMUTOFF  (COL  14)
                                          YES
                                          NO
                                    EXHAUST SYSTEM TYPE  (COLS 27-28),

                                     (COLS 29-30),(COLS  31-32),

                                     (COLS 33-34) AND (COLS 35-36)
                                     01
                                     02
                                     03
                                     04
                                     05
                                     06
                                     07
                                     08
                                     09
       AIR INJECTION
       FN01NE MOD
       FULL INJECTION
       OTHER
       THEPMAL REACTOR
       CATALYTIC REACTOR
       TURBOCHARCER
       EXHAUST RECYCLE
       NONE
                                    EVAP SYSTEM TYPE (COLS 47-48)

                                     01   CRAJ.T.CASE
                                     02   CANISTER
                                     03   TANK
                                     04   NONE

                                    ENGINE TYPE (COLS 50-51)
01
02
03
04
05
06
07
OS
09
10
11
I -BLOCK
V- BLOCK
ROTARY
OPPOSED
TURBINE
EX (STEAM)
EX (FREON)
DIESEL
STIRLING
ELECTRIC
STPATIFIED
                                   CRANKCASE  SYSTEM TYPE  (COL 53)

                                      1    CLOSED
                                      2    OTHER

                                   FUEL TYPE  (COLS  55-56)

                                    01    INDOLENE  30
                                    02    COMMERCIAL LEADED
                                    03    LPG
                                    04    PROPANE
                                    05    OTHER
                                    06    1HD  IIN'LEADED,  91 OCT
                                    07    IND  I'NLEADFD.  100  OCT
                                    08    ill FUEL Oil.
                                    09    12 FUEL OIL
                                    10    NATURAL CAS
                                    11    ALCOHOL
                                    12    INDOLENE  10
                                    13    INDOLENE 20
                                    14    JP-4
                                    15    KEROSENE
                                    16    COMMERCIAL UNLEADED

                                   MAINTENANCE CODE (COL 61)
  1   BEFORE
  2   AFTER
  3   NORMAL

ODOMETER CODE  (COL 62)

  1   MILES
  2   KMS

CARD 6

MANOMETER UNITS (COLS 43-44)
 IN
 CM
 MM
INCHES
CENTIMETERS
MILLIMETERS
Form  707-01   (cont.)

-------
 TFST tfo.
                       CO
MM
SAW
                       CO
 &/
-------
UST »   16-7167
1<57S
                                                         COiSTANT-VOl UMt SA'IPI.FH  RfSULTS
                                                                                                   PROCESSED:   14«38:.43   JAN  3.  1975
COOK MODEL
9^9 TCS CRICKET
A y i p" M / \t
VF.HICLF. I
776-DUZ
** * L tv/v ••' *• TI i j
RATIO RATIO MOPF. STROKE C.


i'

0.0 ' 0.
t-KOUESTOR
NIT. qp/VNCH

0 0.0 0.
0 0.
MOO. INERTIA CURB UO. ACTUAL
.1). YR DTSPI.. WE.KiHT WMGHr CYL. H.P. DYNO.H.P.
/ 72 14J.O 2500 0 •» 0 0.0
FAPTllUP "'5Cf*C " Tc\trry . liAMiirTAr-Tiiuirr C\»TA
r*jv^iu"r. . . r. \*j
(<. TIC I MS
0 0.0
• IL/C.*~~~~'"'MI<*lJ*«V*i»jrfC. U»*l«-" —
PPM % CO GEAf RR-1 HC CO NOX
0. 0.
FUFX
1 DATE
0- 0-
INJ.
0 0
0 0.
EXHAUST S'STEM
SHUT. *CARB SH9LS CARP MODEL TY!1fS 'JAM£
0 0
0
0
0000
').0 0
.0 0.0
EVAP EGN CHAN*
SYS

. TYPE CASE
000
F«pfr

WFT CVS
2".H6 76.0 57.0 100.0
DILUTION
CALCULATED Nnx

'V
0.2'OT4 1^68.
PAG
1 3.590
MILFS
123MH.
FACTOR
O.AS93
COUNTS
FXHiUST SAMPLE


CV3
f

HAG

HC-FIO
CO
C02
NOX CHFM
2 3.910
RANGE
a
5
j>
<•
MILFS
HP TEH
41.6
If .9
35.4
37.3
21122.
CO'-fT.
125.36
41. 79
0 . 952
37.30
COUNTS
EXHAUST SAMPLE






BAG

HC-FIO
CO
CO?
NOX CHFM

3 3.590
RANGE
^
3
2
3

MILES
Mf.TFR
19.2
6.3
22.4
39.8

1.1099.
CONC.
57.11
2. HO
0.584
19.90

COUNTS
AIR 0.0
IGN
TIMING
00
2710.2 CU.
BACKGROUND
f'ANGF. METFP
4 1.4
5 0.3
2 1.5
4 0.4
4621.1 CU.
BACKGROUND
*ANGt METER
4 '1.5
3 0.1
2 1.3
3 0.8

2*65.8 CU.
EXHAIJCJ SAMPLE PACKGROUNO






HC-FIO
CO
C02
NOX CHE^
WANGF.
4
3
2
4
MtTFt?
33.2
37.1
31.3
34.4
CONC.
99.74
IP. 06
0.831
34.40
RANGE METEP
4 2.1
3 0.0
2 1.4
4 0.4
0.0

SULTS««««


SPtC.GS. UNITS IN OUT
1.75 IM
•
IDLE
RPM * CO GEAR RJM
0. 0.0
FT.
SAMPLE
CONC.
4.14
0.8S
0.0'*1
0.40
FT. 1376
SAMPLE
CONC.
4.4J
0.04
0.035
0.40

N 0
24.

EVAP.
ftS 17.45

LOSS TIRE.
A TEST TEST
C UTL TRANS S.PAT. YEAR TYPE
221 1 75 5
tVAP SI7F RIM CYCLF. CODE
0.0 0 0
FUEL FUEL
TYPE TANK MAlNT OOOM GVW
700 0 0
ENGINE FAMILY J 0 00
CVS HOURS I

•OPER. DRIVER NO. UNIT
CFF TAT 08 7C















GRAMS PRES.
•
D/irA(:TOR=13.
CORRECTED
CONCfNT»ATI )NS
121.5? V-P'1
43.00 PP'1
0.914 
-------
 EPA    TEST   PROCEDURE
                                      Number
                                             TP-708
                                                               Page
                                                          f
                                                         of
  SUBJECT
 HOT SOAK EVAPORATIVE
  Reference  FEDERAL REGISTER, VOL. 39, NO. 101,
 MAY 23. 1974. Sec. 95-075-13 & 21	
                                              Data Form No.
                                              705-01, Sec. IV
  Responsible Organization
 TEST OPERATIONS
  Test Witness/Review
 MANUFACTURER'S REPRESENTATIVE, DATA VALIDATION
  Type  of Test Report
 DATA FORM OUT-PUT

  Report Distribution  MANUFACTURER, QUALITY ASSURANCE,
 DATA VALIDATION, CERTIFICATION BRANCH
                                              Computer Program
                                              SEE COMMENTS
                                              Performance Interval
                                              PER VEHICLE
                                              Supersedes
                                              NEW_	

                                              Superseded by
  REMARKS/COMMENTS

 1.0  EVAPORATIVE DATA ANALYSIS IS ACCOMPLISHED BY SAQF:NEWCVS
                            ORIGINAL RELEASE APPROVALS
  Office
Program Mgmt
Lab Branch
   Section
Quality Assurance
Chief
Signature
Date
                                     REVISIONS
 Change
 Letter
 Description of Change
        Approval
Date
                                       21*5

-------
REVISIONS:

HOT SOAK EVAPORATIVE
TEST PROCEDURE
PROCEDURE NO.
TP-708
PAftF , 2 , OF 5
1.0  PURPOSE

     To measure and quantify hydrocarbon evaporative losses after vehicle has
     been driven and is parked in soak area.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Certification Test Vehicle.

3.0  REFERENCES

     3.1  Federal Register, Vol. 39, No. 101, May 23, 1974, Sec. 85.075-13,
          85.075-21.

     3.2  EPA Training Manual, "Light Duty Certification Testing Procedures."

4.0  REQUIRED EQUIPMENT

     4.1  Drying tubes - 3/4 in. ID, tubular, transparent

     4.2  Desiccant, 8 mesh

     4.3  Collection tubing, stainless or aluminum, 5/16 ID.

     4.4  PVC tubing, 5/16 ID.

     4.5  Hosecock clamps, rubber plugs, aluminum foil, tape

     4.6  Balance - accuracy +^075 grams

     4.7  Temperature recorder, multi-channel, range 50  to 100 F, accuracy +1 F

     4.8  Type "J" thermocouples, iron-constantine

     4.9  Carbon traps, activated carbon, 300 +^25 ml, capacity 150 gms activated
          carbon

5.0  PRECAUTIONS

     5.1  Do not place canisters on the floor, or suspend from collection tubing.
          DO NOT KINK LINES.

     5.2  Close the hood as soon as possible after plumbing and collection
          canisters have been reinstalled.

     5.3  Caution should be exercised when connecting and removing canister to
          prevent vapor loss.
                                     247

-------
REVISIONS:
                              HOT SOAK EVAPORATIVE
                          TEST    PROCEDURE
PROCEDURE NO.
    TP-708

PAGE J— OF JL-
 6.0  VISUAL INSPECTION

      6.1  inspect all plumbing and electrical  connections.

 7.0  TEST ARTICLE PREPARATION

      7.1  Re-seal all orifices and vents as  described in section  7.0 of
           procedure TP-^705.

      7.2  Plug exhaust pipe.

      7.3  Re-seal fuel cap area.

      7.4  Reconnect temperature recorder and thermocouple lead  -channel 2 for
           ambient temperature.

      7.5  Check the above  items off in section IV of form #705-01.

-------
REVISIONS:
                              HOT SOAK EVAPORATIVE
                           TEST    PROCEDURE
PROCEDURE NO.
    TP-708	
PAGE_1_OF __5_
 8.0  TEST PROCEDURE

      The following steps are necessary to  assure proper collection of  the hot soak
      evaporative losses.  As each step is  completed check off on form  705-01,
      sec. IV.

 Test Sequence            Test Description                             Data Output

      101      Immediately after the engine  is turned off
               reconnect the carbon canisters to the required
               trap points.  Ref: TP-705.

               NOTE:  Same canisters and placement as in diurnal evap.
                      Remove clamps.

      103      Start one hour soak and record start time.             Start time

      104      Record ambient temperature  at beginning of soak.        Start temp.

      105      Check ambient temperature at  15 min. intervals         Check temp.
               to insure "out of spec" conditions do not occur.

      106      At the end of the one hour  soak record end time        End time
               and final ambient temperature.                         End temp.

      107      Shut off temperature recorder                         Shut off
                                                                     recorder

      108      Reclamp canisters and remove.

      109      Weigh the canisters with hose-cock clamp connected     Hot weight
               and record on form 705-02 in  hot soak wt. block.

-------
REVISIONS:

HOT SOAK EVAPORATIVE
TEST PROCEDURE
PROCEDURE NO.
TP-708
PAGE 5 OFj —
9.0  DATA INPUT

     9.1  Complete section IV of form 705-01 (Vehicle Test and Evap.)  and sign/date
          at the bottom of form.

     9.2  Insure that final hot weight is recorded on form 705-02 (Evap. Emission
          Data).

     9.3  Fold temperature trace and turn in to Data Validation with the above-
          mentioned forms.

10.0 DATA ANALYSIS

     10.1 Subtract the "initial weight" for each canister from the "hot weight" and
          add the "evap. emissions" of each together to get the "Total Evap.
          Emissions."

11.0 DATA OUTPUT

     11.1 Total Evaporative Emissions from the diurnal and hot soak tests.

     11.2 Record on data sheet 707-01.

12.0 ACCEPTANCE CRITERIA

     12.1 The soak time for evap.  collection is not to exceed 1 hour.

     12.2 The ambient temperature must remain between 76 F and 86 F during col-
          lection period.

     12.3 The collection procedure must have been performed correctly.

13.0 QUALITY PROVISIONS

     13.1 Form #705-01 has a built in Quality check in Section IV.  Each step per-
          formed is checked off by the technician and then checked and signed
          off by a witness, thus an audit is performed at the site of the test.

     13.2 The soak time and temperature should be audited by the Q.A.  department
          to assure the specific limits have not been exceeded.

     13.3 If "out of spec" conditions are discovered a request for corrective
          action should be submitted to Test Operations.
                                      250

-------
                     VEHICLE TEST AND EVAPORATIVE DATA


Vehicle Mfgr.	 No.
Inertia Wt . HP A/C Test *

I. HEAT .BUILD ' TECH

A. Drain fuel
B. Plumb air cleaner

C. Plumb canister

D. Plumb bowl vent (if required)

E. Trap gas cap (if required)

F. Seal orifices/vents

G. Install carbon traps (record on data sheet)

H. Hook-up temperature recorder

I. Hook-up thermocouple leads

J. Install heat blanket
•
K. Plug in fuel tank heater (when used)

L. Refuel vehicle - 40% of tank capacity
Tech. Sig. Witness Sig.
M. Replace fuel cap, plug exhaust pipe(s) Unclamp canister
Heat Build Fuel Temp. Fuel Temp. Ambient
Progress Lead No. 1 Lead No. 4 Temp.
0-Min.
15-Min.
30-Min.
45-Min.
6 0-Min.

II. DYNAMOMETER WARM-UP/SET
A. Drive non-test vehicle onto dyno B. Hook-up vehicle as
C. Set inertia lbs.0 H.P. D. Drive @50mph steady
H. Remove vehicle from dvno
I. Tech. Sig. Date
n

D
D

D

n

D

n
i— i
n

n

u

D

D


D









for
st


CTA
n

D
n

D

D

n

n

D

D

n

n

D


D









Hot LA-'!
ate


II. Tech. Sig. Date
                                   251
  FORM 705-01

-------
                                                             FORM 705-01. (Cent,.)


III.   MASS- EXHAUST EMISSIONS .TEST

      A.  Check Varian   Paper-OKD Pen-OKQ Ink-OKO  Zero-OKD

      B.  Cooling fan in place   OK Q Release dyno brake-OK  O

      C.  Hook up     Chock blocks-OKD  Cable winch rj  Exhaust Q

      D.  Temp, recorder   Connect thermocouple leadsQ Start  recorder rj

      E.  CVS    Check fan opcrationQ Bags-OKD Rev. Ctr. Zero Q
                 Leak check-OK G      CVS Temp-OK D
                 Cell temp-OK  G      Return to sample  rj

      F-  Drive test trace  Q     Check tire pressure  (45 PSI)   D

      G.  Remove vehicle to Soak Area  D
                           J                                          '•
 IV.   HOT SOAK EVAPORATIVE EMISSION'S TEST                        TECH   CTA

      A.  Reseal orifices/vents                                   rj    rj

      B.  Reconnect carbon canisters and unclamp                       '-'

      C.  Reconnect temp,  recorder and thermocouple leads         D    D

      D.  Check gas cap                                           r->    p.

      E.  Plug exhaust pipe(s)                                    D    D

      F.  1-hour soak  Start time	 End	                p    p

      G.  Start amb. temp.	 End amp.  temp.	            Q    p

      H.  Check ambient temp, at 15-min. intervals               rj    n.

      I.  End of hot soak  - reclamp canisters and remove         D    D

      J.  Shut-off temp,  recorder                                ._.

      K.  Weigh canisters  and record on data sheet              ,-,   n

  V.   DE-PREP AND VEHICLE  REMOVAL

      A.  Remove all collection tubing, exhaust pipe plug(s),
          orifice/vent plugs, tape, foil,  etc.                   Q   rj
      B.  Disconnect temp, recorder § thermocouple leads        Q    p
      C.  Return engine to Mfgr's running  configuration         D    D
      D.  Move vehicle to  East  lot - keys  to Prod. Contr.       n    m
      E.  "VOID" or "FAILED" vehicles - check with Team Leader
          for disposition
      F.  Leave as is, if  acceptable for IIWFET
III.   Tech.  Sig.	            	 Date	
 IV.  Tech.  Sig.	Date_
                                        252
  V.  Tech.  Sig.	 Date_

-------
            EVAPORATIVE EMISSION WEIGHING  DATA
     TEST NO.
     DATE
     MAKE OF CAR
CANISTER NO.
CANISTER LOCATION
HOT SOAK WEIGHT
INITIAL WEIGHT
EVAP. EMISSIONS





i i














     TOTAL EVAP. EMISSIONS
FORM 705-02
                              253

-------
 EPA    TEST   PROCEDURE
                                      Number
                                             TP-709
                                              Page
                         of
 SUBJECT
 VEHICLE DE-PREP AND REMOVAL
  Reference
 EPA, ANN ARBOR, DRAFT "LIGHT DUTY TEST OPERATIONS"
                                              Data Form No.
                                              705-01 SEC.V,  709-01
  Responsible Organization
 TEST OPERATIONS
                                              Computer Program
                                              NONE
 Test Witness/Review
 TECHNICIAN/CHECKER, TEAM LEADER
                                              Performance Interval
                                              PER VEHICLE
  Type of Test Report
 DATA FORM OUT-PUT
                                              Supersedes
                                              NEW
  Report Distribution
 QUALITY ASSURANCE, DATA VALIDATION, TEST FILE
                                              Superseded  by
  REMARKS/COMMENTS
                            ORIGINAL RELEASE APPROVALS
 Office
Program Mgmt
Lab Branch
Lab Branch
   Section
Quality Assurance	
Chief
Test Operations Chief
Signature
Date
                                    REVISIONS
 Change
 Letter
 Description of  Change
        Approval
Date

-------
REVISIONS:

VEHICLE DE-PREP AND REMOVAL
TEST PROrFDllPF
PROCEDURE NO.
TP-709
PAfiF 2 OF 4
1.0  PURPOSE
     To restore vehicle to Manufacturer's running condition following the FTP
     and Evap. tests and assure correct disposition of the vehicle.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Manufacturer's certification vehicle.

3.0  REFERENCES

     3.1  EPA, Ann Arbor, Draft "Light Duty Test Operations."

4.0  REQUIRED EQUIPMENT

     NONE.

5.0  PRECAUTIONS

     5.1  Care should be taken to assure that all equipment has been re-connected
          correctly.

6.0  VISUAL INSPECTION

     6.1  Check for any collection equipment that may have been overlooked
          during removal.

7.0  TEST ARTICLE PREPARATION

     NONE.
                                     255

-------
REVISIONS:
                           VEHICLE DE-PREP AND REMOVAL
                          TEST    PROCEDURE
                                            PROCEDURE NO.
                                                TP-709	

                                            PAGEJL-OF J__
 8.0  TEST PROCEDURE

      The following steps are required to  assure proper de-prep removal of the
      test vehicle.  Check off items in section V of form #705-01 as  completed.
 Test Sequence

      101
      102
      103
      104A
     Test Description

Remove the following articles
from the vehicle:
o    Collection tubing
o    Exhaust plug  (s)
o    Orifice/vent plugs
o    Tape

Disconnect temperature recorder
and thermocouples.

Return to manufacturer's running
configuration.

If the test is acceptable, move vehicle
to parking lot and return keys to
Production Control.
Data Output

     A.
                                                                         B.
                                                                         C.
                                                                         D.
      104B
      104C
If the test  is  "void" or vehicle "fails"
check with Team Leader for instructions.

Leave vehicle in soak area if HWFET
is to be run.
                                                                         E.
                                                                         F.
                                      256

-------
REVISIONS:

VEHICLE DE-PREP AND REMOVAL
TFST PPOrFHUPF
PROCEDURE NO.
TP-709
PArtF 4 OF 4
9.0  DATA INPUT

     9.1  Section V of form #705-01 is completed and submitted to Data Analysis.

10.0 DATA ANALYSIS

     None required.

11.0 DATA OUTPUT

     11.1 Form is filed with the vehicle data with Data Validation.

12.0 ACCEPTANCE CRITERIA

     12.1 Technician must sign form to verify tasks have been completed.

13.0 QUALITY PROVISIONS

     13.1 A checker will witness all tasks completed by the technician,  thereby
          performing an initial audit of the data sheet.

     13.2 Final test disposition shall be indicated on the data sheet.

     13.3 If the test was void, a failure report (Test Condition Report,
          form #709-01) shall accompany the test data sheet and the type
          of failure should be coded in the space provided.
                                      257

-------
VEHICLE TEST AND EVAPORATIVE DATA



                          No.
Inertia Wt . HP A/C Test 0

I. HEAT -BUILD

A. Drain fuel
B. Plumb air cleaner

C. Plumb canister

D. Plumb bowl vent (if required)

E. Trap gas cap (if required)

F. Seal orifices/vents
G. Install carbon traps (record on data sheet)

H. Hook-up temperature recorder

I. Hook-up thermocouple leads

J. Install heat blanket
'
K. Plug in fuel tank heater (when used)

L. Refuel vehicle - 40% of tank capacity
Tech. Sig. Witness Sig.
TECH
D

a
a

a

D

a

D
D

D

a

a

D


M. Replace fuel cap, plug exhaust pipe(s) Unclamp canister [J
Heat Build Fuel Temp. Fuel Temp. Ambient
Progress Lead No. 1 Lead No. 4 Temp.
0-Min.
15-Min.
30-Min.
45-Min.
60-Min.

II. DYNAMOMETER WARM-UP/SET
A. Drive non-test vehicle onto dyno B. Hook-up vehic
C. Set inertia lbs.0 H.P. D. Drive OSOmph
h. Remove vehicle from dvno
I. Tech. Sig. Date









CTA
D

D
D

a

D

a

n
a

D

a

a

D


a









le as for Hot LA-'i
steady state


II. Tech. Sig. 258 Datc
TTT1T7M TOR m • 	 __

-------
                                                         FORM 705-01 (Cont.)



III.   MASS  EXHAUST EMISSION'S TEST

      A.  Check Varian   Papcr-OKQ Pen-OK Q Ink-OKQ  Zero-OKQ

      B.  Cooling fan in place   OKQ Release dyno brakc-OK O

      C.  Hook up     Chock blocks-OKQ  Cable winchQ  Exhaust D
                 t
      D.  Temp,  recorder   Connect thermocouple leadsQ Start recorder Q

      E.  CVS     Check fan opcrationQ Bags-OKQ Rev.  Ctr. Zero D
                 Leak check-OK G      CVS Temp-OK Q

                 Cell tcmp-OK  [j      Return to sample n

      F.  Drive test  trace  Q     Check tire pressure (45  PSI)   O

      G.  Remove vehicle to Soak Area
 IV.   HOT  SOAK  EVAPORATIVE EMISSION'S TEST                       TECH  CTA

      A.   Rcseal  orifices/vents                                  Q     Q

      B.   Reconnect  carbon canisters and unclamp                 ^     '-'

      C.   Reconnect  temp,  recorder and thermocouple leads        D    D
u . unecK yub cup
£. Plug exhaust pipc(s)
F. 1-hour soak Start time End
G. Start amb . temp. End amp. temp.
H. Check ambient temp, at 15-min. intervals
I. End of hot soak - reclamp canisters and remove
J. Shut-off temp, recorder
K. Weigh canisters and record on data sheet
V. DE-PREP AND VEHICLE REMOVAL
A. Remove all collection tubing, exhaust pipe plug(s),
orifice/vent plugs, tape, foil, etc.
B. Disconnect temp, recorder f, thermocouple leads
C. Return engine to Mfgr's running configuration
D. Move vehicle to East lot - keys to Prod. Contr.
E. "VOID" or "FAILED" vehicles - check with Team Leader
for disposition
F. Leave as is, if acceptable for IIWFET
III. Tech. Sig. Date
IV. Tech. Sic- Date
259
V. Tech. Sic. Hate
D D
D D
n n
D n
n D
n D
n n
D n


n n
D n
D n
n n







-------
                         TEST  CUNUI'l UJN RLl'ukT

Failure              Void  	       Retcst Requested
Name                        	  Date Submitted
Branch                    Section	 Extension
Test Type:  	 LD       	 MD      	 HD      	 Other

Manufacturer                       Identification Number 	
Date           Time 	    Operator
Equipment  Involved  in  Failure:

	 Analysis  System       	 Recorder         .   Bags

	 HC      	 CO       	 NO      	 CO2      	 Temp

      CVS            Drivers Trace            FID
       CVS  Counter       	 Cold  Start      	 Hot Start

       Dynamometer       	 Other (Specify)
 Failure  Description
Void Point	Hours  Lost	
(:.                                             (Include Prep TfmeT

Corrective Action Taken	
cc:  D.  Clark
    M.  Uavis
    Jesse MeC;i 11
    Team Loader
                                                             2/8/74
                                    260
   FORM 709-01

-------
EPA TEST
PROCEDURE
Page l of «
SUBJECT
HIGHWAY FUEL ECONOMY PRE-CONDITIONING
Rpfprpnrp FEDERAL REGISTER, VOL.39,
APPENDIX "EPA REC PRAC FOR COND HIWA
Responsible Organization
TEST OPERATION
Test Witness/Review
MANUFACTURER'S REPRESENTATIVE, TEAM
Type of Test Report
DATA SHEET
Report Distribution
QUALITY ASSURANCE, CERT. BRANCH, DATA
NO. 200, OCT. 15, 1974- Data Form No.
Y FUEL ECON TESTS" 710-01
Computer Program
NONE
Performance Interval
LEADER PER VEH, AS REQ
Supersedes
NEW
Superseded by
VALIDATION, TEST FILE
REMARKS/ COMMENTS
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Branch
Lab Branch


Section
Quality Assurance
Chief
Signature


Test Operations Chief


Date





REVISIONS
Change
Letter
Description of Change Approval

Date

261

-------
REVISIONS^


HIGHWAY FUEL ECONOMY PRE-CONDITIONING
TEST PROCEDURE
PROCEDURE NO.
TP-710
PAGE 2 OF 4

1.0  PURPOSE

     To prepare vehicles for the 1975 Highway Fuel Economy Test.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Test vehicle designated for the HWFET.

3.0  REFERENCES

     3.1  Federal Register, Vol. 39, No. 200, Oct. 15, 1974 - Appendix "EPA
          Recommended Practices for Conducting Highway Fuel Economy Tests"

4.0  REQUIRED EQUIPMENT

     4.1  Chassis dynamometer and associated meters.

     4.2  Driver's aid - Hewlett-Packard, Varian.

5.0  PRECAUTIONS

     5.1  Insure proper fuel is used.

     5.2  Inertia setting and horsepower and shift points  (unless specified)
          are the SAME AS_ THE FTP.

6.0  VISUAL INSPECTION

     6.1  Check the vehicle set-up.

7.0  TEST ARTICLE PREPARATION

     7.1  Drive the vehicle from the soak area and onto the dynamometer.

     7.2  Tie-down vehicle with winch cable(s), place fan 12 inches in front
          of grill and hook-up exhaust vent system.
                                        263

-------
REVISIONS^
                       HIGHWAY FUEL ECONOMY PRE-CONDITIONING

                          TEST    PROCEDURE
                                                 PROCEDURE  NO.
                                                      TP-710	

                                                 PAGE_LOF J__
 8.0  TEST PROCEDURE

      The following steps must be taken to assure the proper preparation of a
      test vehicle for the Highway Fuel Economy Test.
 Test Sequence
      101
      102
      102A
      102B
      102C
               Test Description

Drive vehicle from soak area immediately following
the "Hot Soak Evap. Test." onto the dyno.  Drive
one-preconditioning HWFET.

In the event the FTP and HWFET cannot be run back to
back, precondition vehicle as follows:

Less than 3 hours  of soak (including 1 hour hot  soak)
Drive one preconditioning HWFET and one for data col-
lection.  Set horsepower prior to warm-up HWFET.

Three to 24 hours  of soak:  Drive 5 minutes at 50 mph
followed by one preconditioning HWFET and one for
data collection.   Set horsepower during the 50 mph
cruise.

Greater  than 24 hours of soak or periods of outdoor
storage:  Run the  "AMA" preconditioning route, an
LA-4 dynamometer simulation, a preconditioning HWFET
and one  for data.  Set horsepower prior to the LA-4.
Data Output
                                      26k

-------
REVISIONS:

HIGHWAY FUEL ECONOMY PRE-CONDITIONING
TEST PROCEDURE
PROCEDURE NO.
TP-710
4 4
 9.0 DATA INPUT

     9.1  Complete data form #710-01 to indicate Preconditioning was completed.

10.0 DATA ANALYSIS

     None required.

11.0 DATA OUTPUT

     11.1 Data form is entered into vehicle file.

12.0 ACCEPTANCE CRITERIA

     12.1 Required preconditioning (see section 8.0)  must be completed and
          documented prior to sample HWFET.

13.0 QUALITY CONTROL PROVISIONS

     13.1 If the required preconditioning has not been performed submit a
          request for corrective action.
                                      265

-------
             HIGHWAY FUEL ECONOMY PRECONDITIONING
                          CHECK SHEET
1.   Check off the box corresponding to the type of HWFET pre-
    conditioning performed.

    /~7  Drive vehicle from soak area and immediately following
         the "Hot Soak Evap.  Test" and onto the dyno.  Drive
         one preconditioning HWFET.

         In the event the FTP and HWFET cannot be run back to
         back, precondition vehicle as follows:

    /~7  Less than 3 hours of soak (including 1 hour hot soak):
         Drive one preconditioning HWFET and one for data
         collection.  Set horsepower prior to warm-up HWFET.

    /~~7  Three to 24 hours of soak:  Drive 5 minutes at 50 mph
         followed by one preconditioning HWFET and one for data
         collection.  Set horsepower during the 50 mph cruise.

    /~7  Greater than 24 hours of soak or periods of outdoor
         storage:  Run the "AMA" preconditioning route, an LA-4
         dynamometer simulation, a preconditioning HWFET, and
         one for data.  Set horsepower prior to the LA-4.
                              Technician
Date:                         and I.D. No.
Time:
Form 710-01

                                266

-------
EPA TES
SUBJECT
HIGHWAY FUEL
T PROCEDURE **" TP-711 paqe l Qf 4
ECONOMY DYNO TEST
Reference Data Form No.
FEDERAL REGISTER, VOL. 39, NO. 200, Oct. 15, 1974 - Appendix 707-01
Responsible Organization Computer Program
TEST OPERATIONS ANALYSIS; SAQF:NEWCVS
Test Witness/Review Performance Interval
MANUFACTURER" S REPRESENTATIVE, DATA VALIDATION PER VEHICLE AS REQ.
Type of Test
DATA SHEET
Report Supersedes
NEW
Report Distribution Superseded by
QUALITY ASSURANCE, DATA VALIDATION, CERT. BRANCH. FILE
REMARKS/ COMMENTS

Office
Program Mgmt
Lab Branch
Lab Branch



Change
Letter

ORIGINAL RELEASE APPROVALS
Section Signature
Quality Assurance
Chief
Test Operations Chief


Date





REVISIONS
Description of Change Approval

Date

267

-------
REVISIONS:


HIGHWAY FUEL ECONOMY DYNO TEST
TEST PROCEDURE

PROCEDURE NO.
TP-711
PAftF 2 OF 4

1.0  PURPOSE

     The Highway Fuel Economy Test is a nonmetropolitan driving cycle, 10.2 miles
     long with an average speed of 48.6 mph.  A vehicle is driven on a dyna-
     mometer following the cycle and emissions are collected by the same means
     as the FTP.

2.0  TEST ARTICLE DESCRIPTION

     2.1  Test vehicle designated for HWFET

3.0  REFERENCES

     3.1  Federal Register, Vol. 39, No. 200, Oct. 15, 1974 - Appendix "EPA
          Recommended Practices for Conducting Highway Fuel Economy Tests."

4.0  REQUIRED EQUIPMENT

     4.1  Constant Volume Sampler equipped to meet requirements in Federal
          Register , Sec. 85.075-20.

     4.2  Chassis Dynamometer

          o    Clayton, Model ECE-50

     4.3  Computer generated driver's aid

          o    Hewlett-Packard, Varian

     4.4  Highway Fuel Economy driver's trace (2 cycles)

5.0  PRECAUTIONS

     5.1  Insure test vehicle is aligned on dynamometer correctly and tied down.

     5.2  It is extremely important that the horsepower/inertia settings used
          for the HWFET are the same as previously used for the FTP.

6.0  VISUAL INSPECTION

     6.1  Insure fan and tail pipe connector(s)  are in place.

     6.2  Check bags for correct installation.

7.0  TEST ARTICLE PREPARATION

     7.1  Follow procedures detailed in procedure TP-707

     7.2  Check driver's aid for paper and ink.
                                      269

-------
REVISIONS:
                         HIGHWAY FUEL ECONOMY  DYNO TEST
                          TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                     TP-711
                                                              4
 8.0  TEST PROCEDURE
      The Highway Fuel Economy data is collected as a result of the following
      procedural steps.
 Test Sequence

      101



      102


      103



      104


      105
              Test Description

Following the preconditioning HWFET,  the  driver
has 15 seconds to prepare for the actual  sample
period.

Two seconds  before the first acceleration the CVS
counter button is depressed to start  the  sample period.

The driver will drive the vehicle in  the  same manner
as required  for the FTP to insure "out  of spec" con-
ditions do not occur.

Two seconds  after the final decel to  zero the rev.
count button is depressed to end the  sample period.

The sample bags are delivered to the  analyzer opera-
tor for analysis.
Data Output
                                     270

-------
REVISIONS:


HIGHWAY FUEL ECONOMY DYNO TEST
TEST PROCEDURE
1 hw 1 1 IXV^ V» ft* U Wl\h
PROCEDURE NO.
TP-711
PAftF 4 OF 4

 9.0 DATA INPUT

     9.1  Fill out form #707-01 and sign off after test completion.

     9.2  Driver will sign HWFET trace.

10.0 DATA ANALYSIS

     10.1 Driver's trace should be checked for "out of spec." conditions.

11.0 DATA OUTPUT

     11.1 Driver's trace and form #707-01 are submitted to Data Validation

12.0 ACCEPTANCE CRITERIA

     12.1 The driver's trace is subject to the criteria of acceptance detailed
          in Section 12.0 of procedure 706.  (Urban Dyno.  FTP)

     12.2 Sample period should be 765 ±2 seconds.

13.0 QUALITY CONTROL PROVISIONS

     13.1 The Quality Control section should inspect the driver's trace to assure
          the acceptable limits stated in Section 12 have been followed.

     13.2 If "out of limits" conditions are discovered, Quality Control should
          implement corrective action.  (i.e., have Production Control
          reschedule vehicle for test.)
                                       271

-------
                                                  CONSTANT VOLUME SAMPLER  (CVS) DATA  SHEET
           MANF.

           CODE
                                               VEHICLE 1.0.
                                                MOD.
                                                 YH
INERTIA

WEIGHT
 CURS
WEIGHT
NO.
CYL.
  5 2 H   I- CC   H UI
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< 3 H Wl   H >
                                                                                                                                     01
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                           10       15       20


                         • MANUFACTURER  SPECS 	
N/V
                                                                     45       50


                                                                  MANUFACTURER DATA
                                                                                                                                 70
                                                                                                                                                  eo
                                                                            IDLE
RATIO


REQU
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                                                                                                       65

                                                                                                   - EPA CODE •
                                                                   80


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ro
LABORATORY COMMENTS







TEST DATE

-


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1 1
75 i 40

-------
EPA TEST
SUBJECT
SAMPLE ANALYSIS
Number
PROCEDURE TP-712
FOR HWFET
Reference FEDERAL REGISTER, VOL. 39, NO. 200, Oct.
APPENDIX, "EPA Rec Prac for Conducting Hiway Fuel E
Responsible Organization
TEST OPERATIONS
Test Witness /Review
TEAM LEADER, QUALITY ASSURANCE
Type of Test Report
COMPUTER PRINT-OUT
Report Distribution
QUALITY ASSURANCE, DATA VALIDATION, CERT BRANCH
Page 1 of l

15,1974 - Data Form No
con Test" 707-01,02
Computer Program
SAQF: NEWCVS
Performance Interval
PER VEH, AS REQ
Supersedes
NEW
Superseded by
REMARKS/ COMMENTS
1.0 The sample analysis of the HWFET is essentially the same as in procedure
TP-707 with the following exceptions.
1.1 Only one background and one sample bag is analyzed. (Bag 1 entry on
form #707-01.)
1.2 CO» will be measured on the upper two-thirds of the selected range.
1.3 Fuel economy is calculated from the composite results using
program SAQF : NEWCVS .
ORIGINAL RELEASE APPROVALS
Office
Program Mgmt
Lab Branch
Lab Branch



Change
Letter
Section Sig
Quality Assurance
Chief
Test Operations Chief


REVISIONS
Description of Change

nature





Date






Approval

Date

273

-------
                                         CONSTANT VOLUME SAMPLER  (CVS) DATA SHEET
   O
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o

o

MANF.
CODE




MODEL





1






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                     • MANUFACTURER SPECS •
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                                                                    MANUFACTURER DATA
 REQUESTOR

INIT. BRANCH
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                                     IGN.
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                                                        35
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                                                                                              65
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   O4-10-74

-------
       CODE  EQUIVALENCE

       CARD 1

       HA.VF CODE (COLS 1-3)

       010   AMERICAN MOTORS
       Oil   (CHRYS) CHRYSLER
       OJ2   (CHRYS) DODGE
       OJJ   (CHRYS) PLYMOUTH
       Oil   (FO MO CO) FORD
       032   (FO MO CO) LINCOLN
       033   (FO MO CO) MERCURY
       041   (CM) BUICK
       042   (CM) CADILLAC
       043   (CM) CHEVROLET
       044   (CM) OLDSMOBILE
       045   (CM) PONTIAC
       046   (CM) CMC
       047   (CM) DETROIT DIESEL
       050   ABARTH
       060   A C CARS
       064   AICHI
       070   ASTON MARTIN
       080   AUTO CAR
       085   AUTO SPORT
       090   ALFA ROKEO
       095   AM GENERAL
       100   AVANTI
       105   AUBURN
       110   AUSTIN MORRIS (BLMC)
       120   BMW
       125   BOLWELL
       130   BRISTOL
       135   BRICKL1N
       140   CHECKER
       150   CITROEN
       160   COMMER
       170   SAMCO (CORD)
       175   DACIA (ARO)
       180   DAF
       190   DAIHATSU
       200   KERCEOES BEHZ
       205   DE TOMASO
       210   DUAL CHAl
       215   DTTNA TRUCK
       220   FERRARI
       230   FIAT
       240   FORD OF ENGLAND
       245   FORD 0? CERMA.VY
       250   HINO
       255   HARLEY-DAVIDSON
       260   HONDA
       270   IHC
       280   ISO
       .290   ISUZU
       300   JAGUAR (BLMC)
       310   JENSEN
       320   JOHN FITCH
       330   JEEP (KAISER)
       340   LANCIA
       350   LOTUS
       360   KASERATI
       365   HOHS
       370   MORGAN
       380   NISSAN
       390   NSU
       400   OPEL
       405   PANTHER
       410   PEUGEOT
       420   PORSCHE
       430   RENAULT
       440   ROLLS-ROYCE
       450   ROOTES
       460   ROVER  (BLMC)
       470   SAAB
       480   SHELBY
       490   MITSUBISHI
       495   SIATRA
       500   SIMCA
       510   SKODA
       520   SS  AUTOMOBILE
       530   TRIUMPH (BLMC)
       535   STUTZ
       540   SUZUKI
       550   TORINO
       560  TOYO KOCYO
       570  TOYOTA
       580  VAUXHALL
       590  VOLKSWAGEN
       600  VOLVO
       605  WHITE
       610  YENKO
       615  YAMAHA
       620  TVR
       630   SUSPENSIONS  INT  (OMEGA)
       640  AUDI
       650  MURENA MOTORS
       660  FUJI HEAVY IND
 CODE   EQUIVALENCE

 670    MONTEVERDI
 680    INTERMECCANICA  (ITALIA)
 690    LAMBORGHINI
 700    MARCOS
 710    ARMY
 720    WIMNEBACO
 725    ALL IS CHALMERS
 730    CATERPILLAR
 740    CUMMINS
 750    HERCULES
 760    MACK
 770    PLRKINS
 180    SCAHIA-VABIS
 790    CLASSIC
 800    TELEDYNE CONTINENTAL
 810    CASE
 820    DIAMOND REO
 830    HIGHWAY PRODUCTS,INC
 999    EXPERIMENTAL

 AIR CONDITIONING (COL 61)
                                                                                         rODE  EQUIVALENCE
  1   WITH
  2   WITHOUT
UTILITY VEHICLE  (COL 62)
      YES
      NO
TRANSMISSION  (COL 63)
      AUTO
      3-SPEED
      4-SPEED
      5-SPEED
      SEMI-AUTOMATIC
SHIFT PATTERN (COL 64)'
  1   STANDARD
  2   OPTIONAL

TEST TYPE  (COLS 69-70)

 00   VOID
 01   CERT (EMISSION DATA)
 02   CERT (DURABILITY)
 03   CCRT (CORRELATION)
 04   SURVEILLANCE
 05   EXPERIMENTAL
 06   FIELD SURVEILLANCE
 07   PARTICIPATES
 08   OTHER
 09   CVS CORRELATION
 10   RESEARCH
 11   CORRELATION (LAB)
 12   CERT (RUNNING CHANCE)

TRAIN (COLS 74-75)

 1-97 AECAS
 98   PARTICULATES
 99   PROP SAMPLER

CARD 2

DRIVING CYCLE (COL 67)
      7-MODE
      LA-4
      LA-4 S3
      ANN ARBOR
      LA-4 S4
      9X7 MODE
      STEADY STATE
      OTHER
SOURCE CODE (COLS 69-70)

 01   MANUFACTURER
 02   HERTZ DETROIT
 03   HERTZ L.A.
 04   AVIS
 05   AIRWAYS CORP L.A.
 06   ALPH CORP L.A.
 07   CSA L.A.
 08   PO DEPT DETROIT .
 09   PO DEPT L.A.
 10   L.A. COUWTY VEH
 11   STATE OF CALIFORNIA
 12   BORROWED FROM CORPS
 13   AMFRICAN RACEWAYS. INC
 14   DEALER USED CARS
 15   EPA
 .16   CSA
 17   MILITARY
  18
  19
 PRIVATE OWNER
 OTHER
 CARD 3
 FUEL INJECTION (COL 13)
       YES
       NO
 FUEL SHUTOFF (COL 14)
       YES
       NO
 EXHAUST SYSTEM TYPE  (COLS  27-28),

  (COLS  29-30),(COLS  31-32),

  (COLS  33-34)  AND  (COLS  35-36)
  01
  02
  03
  04
  05
  06
  07
  08
  09
AIR  INJECTION
ENGINE MOD
FUEL INJECTION
OTHER
THEPMAL REACTOR
CATALYTIC REACTOR
TURBOCHARCER
EXHAUST RECYCLE
NONE
EVAP SYSTEM TYPE  (COLS 47-48)

 01   CRANKCASE
 02   CANISTER
 03   TANK
 04   NONE

ENGINE TYPE (COLS 50-51)
 01
 02
 03
 04
 05
 06
 07
 OS
 09
 10
 11
I-BLOCK
V-BI.OCK
ROTARY
OPPOSED
TURBINE
EX  (STEAM)
EX  (FREON)
DIESEL
STIRLING
ELECTRIC
STRATIFIED
CRANKCASE SYSTEM TYPE (COL 53)

  1   CLOSED
  2   OTHER

FUEL TYPE (COLS 55-56)

 01   INDOLENE 30
 02   COMMERCIAL LEADED
 03   LPC
 04   PROPANE
 05   OTHER
 06   IND UNLEADED, 91 OCT
 07   IND TO.EADED, 100 OCT
 08   II FUEL OIL
 09   n FUEL OIL
 10   NATURAL CAS
 11   ALCOHOL
 12   INDOLENE 10
 13   INDOLENE 20
 14   JP-4
 15   KEROSENE
 16   COMMERCIAL UNLEADED

MAINTENANCE CODE (COL 61)

  1   BEFORE
  2   AFTER
  3   NORMAL

ODOMETER CODE (COL 62)

  1   MILES
  2   KMS

CARD 6

MANOMETER ITOITS (COLS 43-44)
 IN
 CM
 MM
INCHES
CENTIMETERS
MILLIMETERS
Form  707-01  (cont.)
                                                        275

-------
 resr tfo.
              R
CO
Bfa
       //&
CO
A
5/4
fi/?
                               276
     form 707-02

-------
    TEST «  16-71iS7

    MFG.
   CODE      MOOKL
    >>99  TCCS CWICK5T
                                              197S
                                              FUEL  ECONOMY  CYCLE
                                                                                  PROCESSED!   14:25t4fe
                                                                                                             3, 19T5
              VFHICLf
              776-OU/
                                  I.D.
                            MOD.
                                         72
        OISPL.
        1M.O
INF.RTIA
WFTGHT
 2500  '
 CUPR
WF.IGHT
   0
 NO.
CYL.
 4
H.P.
  0
 ACTUAL
DYNO.H.P.
  0.0
A
C
2
UTL TRANS S.PAT.
 2    1     1
TEST
YEAR
 75
TEST
TYPE
 5
TEST DATE
 1- 1-75
ODOMETFS
   603*.
                         IND.     KAPO   / ---- TEMP., OF -------- / ---- MANOMFTEF --- / ----- CVS PREP. ---- / --- INITIALS --- /   DYNO. CVS
                         H.P.     "HO       ORY     WFT     CVS     SPEC.GR.  UM T 5     IN     DOT       OPER.  DRIVER     NO.  UNIT
                          6.2     ?fl.*6     7^r.4   57.7    99. S      1.75    Ilv       24.90   17.25      CFJ     TAT      08    7C
                             DfLUTION AIR    0.0    0.0                              '  '
     CU^IC FT
     PER t^EV.
      0.270?B
   CALCULATED
      PPM
                              NOX
                            FACTOR
                            o.flsoa
  IGN                          IDLE   F.VAP. LOSS  TIME
TIMING    PPM   -5 CO   GEAR     RFM      GRAMS    PRES,
           0.   0.0               0.     AA.AA    45.0
HAG 1    10.225 MILES    1^30. COUNTS
                  FXHAUST SAMPLE
                          4073.5  CU.  FT.
                                                       765.3 SECONDS  0/FACrOW=10.192 ACT PPM» 1460.6 RPM RATIO(C/A)=0.9953

HC-FID
CO
CO?
NOX CMEM
RANGE
4
3
2
4
Mf TER
33. fl
20.5
46.2
56.2
CONC. 1
101 ,S6
9.bl
1.304
56.20
4ANI
4
3
2
4
                          RACKGROUND SAMPLE
                                METER   CONC.
                                 1.7   ' 5.02
                                 0.0    0.0
                                 1.5    0.041
                                 0.5    0.50
                     CORWtCTFD
                   CONCENTRATIONS,
                      97.03 PPM "    6.45
                       9.61 PPM      1.29
                       1.267 .*    2676.08
                      55.75 PPM     10.46
                                                                             MASS-EMISSIONS
                                                                                     GMS/MI       MPG1
                                                                                      0.63
                                                                                      0.13 '
                                                                                    261.72       33.6
                                                                                      1.02
   ro
   -a
   —Q
                                                                                                                                     ft
                                                                                                                                     0)
                                                                                                                                     o
                                                                                                                                     n>
                                                                                                                                     3
                                                                                                                                     rt-
                                                                                                                                     2!
                                                                                                                                     o

-------
800

-------
  Section 800
DATA VALIDATION
       279

-------
EPA TEST PROCEDURE NUmber Tp-801
Page 1 of n
SUBJECT
DATA VALIDATION
Reference
EPA, ANN ARBOR, DRAFT "LIGHT DUTY TEST OPERATIONS
Responsible Organization
TEST OPERATIONS
Test Witness /Review MANUFACTURER'S REPRESENTATIVE/
CERTIFICATION BRANCH REPRESENTATIVE
Type of Test Report FINAL COMPUTER OUT-PUT OF EMISSION
DATA AND COMPILED VEHICLE FILE
Report Distribution QUALITY ASSURANCE, CERTIFICATION
BRANCH, MANUFACTURER'S REPRESENTATIVE, TEST OPERATIONS,
Data Form No.
SEE SECTION 2.0
Computer Program
SEE SECTION 10.0
Performance Interval
PER VEHICLE
Supersedes
NEW
Superseded by
REMARKS/ COMMENTS DATA VALIDATION, PRODUCTION CONTROL

Office
Division Dii
Lab Branch
Lab Branch



Change
Letter

ORIGINAL RELEASE APPROVALS
Section Signature
:ec Quality Assurance

Chief
Test Operations Chief


Date





REVISIONS
Description of Change Approval

Date

281

-------
REVISIONS:

DATA VALIDATION
TEST PROCEDURE
PROCEDURE NO.
TP-801
PAftF 2 op 11
 1.0 PURPOSE

     Data Validation establishes a control network to assure a smooth flow of
     all data collected from Production Control  (scheduling) and Test Operations
     (Acceptance, Pre-conditioning/Prep, FTP and HWFET).  The Data Validation
     section will also check the data form to confirm the validity of the results
     and assure the data is within specified limits.

2.0  TEST ARTICLE DESCRIPTION

     2.1  The following data sheets, chart traces and reports are required for a
          complete Data Validation system.

               o    Form 701-01, Driver's Preconditioning Report.
               o    Form 705-01, Vehicle Test and Evaporative Data Sheet
               o    Form 705-02, Evaporative Emissions Data Sheet
               o    Form 707-01, CVS Data Sheet
               o    Form 707-02, Analyzer read-out  (FTP and HWFET)
               o    FTP driver's trace
               o    FTP analyzer traces
               o    CVS temperature trace
               o    Diurnal temperature trace
               o    Preliminary results
               o    Official values (1 each)
               o    Official values (2 each)
               o    CVS Data Sheet (blue copy), form 707-01
               o    Form 707-01, HWFET CVS Data Sheet
               o    HWFET re-test  (if necessary)
               o    HWFET clearance
               o    HWFET driver's trace
               o    HWFET preliminary results
               o    Form 801-01, Weekly activity report
               o    Data processing job request

3.0  REFERENCES

     3.1  EPA, Ann Arbor, Draft, "Light Duty Test Operations"

     3.2  "Test Validation Procedures," Joe Belanger, EPA, Ann Arbor,
          30 September 1974.

4.0  REQUIRED EQUIPMENT

     4.1  Validation stamps

5.0  PRECAUTIONS

     5.1  Not applicable.

6.0  VISUAL INSPECTION

     6.1  Contained in Section 8.0

-------
REVISIONS:
                             DATA VALIDATION
                        TEST    PROCEDURE
PROCEDURE NO.
    TP-801

PAGE_2
 7.0  TEST ARTICLE PREPARATION

     7.1  All forms and traces must be complete before submittal to Data
          Validation.
                                 284

-------
REVISIONS:

DATA VALIDATION
TEST PROCFDUPF
PROCEDURE NO.
TP-801
PAC,F 4 OF 11
8.0  TEST PROCEDURE

     The procedures for Test Data Validation serve a multi-purpose.  First, they
     illustrate the functional flow of the paperwork system and the sequence of
     tests.  Finally, it is a system for checking the validity of the test data
     itself.

     The procedures are divided into five sections, in order to ease interpretation
     of the sequence.  Each section has a mini-flow diagram to further illustrate
     the steps to be followed.
                                  SECTION I
                       CERTIFICATION
                          BRANCH
             DATA
          VALIDATION
           CANISTER
           WEIGHER
Test Sequence
     101
     102
     103
                        PRODUCTION
                          CONTROL
                                                   A. Form 705-01

                                                   B. Form 701-01

                                                   C. Form 707-01

                                                   D. Form 705-02
                         VEHICLE
                           PREP
             HEAT
            BUILD
     104
                Test Description

 Certification Branch representative and the
 Manufacturer's Representative initiate a test
 request.

 The request (CVS data sheet)  is sent to Production
 Control for scheduling.

 The CVS Data Sheet (707-01)  are picked up daily
 from Production Control by the Data Validation
 section along with the daily test schedule and
 test number assignments.

 The following information is recorded on form #707-01
 by Data Validation and the form is placed on the
 corresponding test vehicle.

      o    Date
      o    Odometer reading
      o    Manometer specific gravity
      o    Test cycle  mileage(s)
      o    Tire pressure
      o    Timing,  RPM,  % CO  (idle)
	and idle RPM	

                       285
Data Output

-------
REVISIONS:
                                 DATA VALIDATION
                          TEST    PROCEDURE
                                                               PROCEDURE  NO.
                                                                   TP-801	

                                                               PAGEJL.OF _ii_
Test Sequence

     105


     106
              Test Description

The test number is also recorded on forms #701-01,
705-01 and 705-02.
               Twenty copies of the  daily schedule are distributed
               as follows:

                    o    1 copy each:  Data Branch
                                      Certification Branch
                                      Team Leaders
                                      Each Analyzer Train
                                      Posted on Soak billboard

                    o    1 copy and  the original to Production
                         Control.

                    o    3 copies  remain in Data Validation

                    o    7 copies  to lab technicians
                                                                Data Output
                                  SECTION II
                                                           A.- D. See Sec. I

                                                           E .  Driver ' s Trace

                                                           F.  Analyzer Traces

                                                           G.  Form 707-02

                                                           H.  CVS Temp. Trace

                                                           I .  Diurnal/Hot
                                                              Soak Trace (s)
 Test Sequence

      201
                             Test Description

              During the 1975 Mass Emissions Test,  the  CVS
              Operator records the following on form #707-01,

                   o    Indicated horsepower

                   o    Barometric pressure
                                                Data Output
                                                                hp

                                                               Baro.
                                     286

-------
REVISIONS:
                                  DATA VALIDATION
                           TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                     TP-801
                                                 PAGEJL_OF
                                                                             11
  Test Sequence
       202
       203
      204
                   Test Description

     o    Wet and Dry bulb temperature

     o    CVS temperature

     o    CVS pump  inlet and outlet pressure

     o    Operator  and driver's initials

     o    Rev.  counts and seconds

     o    CVS hours

     o    Analyzer  train number

The driver's trace  and analyzer traces generated
during the test are checked by the Manufacturer's
Representative and  the Certification Branch rep-
resentative and signed as '"valid" or "invalid."

The CVS.operator delivers the traces and form
707-01 to Data Validation.

Following the Mass  Emission Test and hot soak
evaporative, the remaining documentation is taken
to the canister weigher.  After recording evap.
results,  he delivers all documentation to Data
Validation.
                   SECTION III
                                 C,E,F,G,HJ
                             DATA
                          VALIDATION
           PRODUCTION
             CONTROL
                          CERTIFICATION
                             BRANCH
          Data Output
                                                                     V °B

                                                                     Inlet Temp.
                                                                     P    P
                                                                      IN'  OUT

                                                                     Initials

                                                                     Revs, Sees

                                                                     Hours

                                                                     Number
                                                                     Valid
                                                                     Invalid
           CERTIFICATION
             BRANCH
A. - I.  See  Sec. I
        and  II

J. Preliminary
   Results

R. HWFET Clearance
                             DATA
                          VALIDATION
                              T
                                       287

-------
REVISIONS:
                                 DATA VALIDATION
                           TEST    PROCEDURE
                                                 PROCEDURE NO.
                                                      TP-801
                                                 PAGE—Z-OF
                                                                              11
 Test Sequence
      301
      302
      303
                    Test Description

Data Validation receives all documentation
from the CVS operator  and canister weigher
following the FTP  and  makes a file envelope
for each test.

The analyzer traces  are checked for proper procedure
and the chart values are compared with those logged
on the analyzer read-out form.

The concentration  values are transcribed onto the
CVS data sheet and all other entries are audited
for obvious errors.
Data Output
      304       The CVS data  sheet is taken to the Data Branch
                (data processing job request required)  for pre-
                liminary result analysis.

      305       The Certification Branch representative obtains
                the CVS data  sheet and preliminary results from
                the Data Branch.  The results are checked and
                if it is a  data vehicle, Production Control is
                given clearance for the HWFET.  The representative
                then logs HWFET at bottom of CVS data sheet.

      306       After the preliminary results and form #707-01
                (CVS)  is received from the Certification Branch
                representative, Data Validation section compares
                the results of the preliminary print-out with the
                analyzer read.  Errors, if any, are corrected
                and the corrected data sheet is re-routed to the
                Data Branch for a new print-out.

      307       Data Validation checks off the remaining docu-
                mentation and places it in the appropriate file.
                                      288

-------
REVISIONS:
                                 DATA VALIDATION
                           TEST    PROCEDURE
                                                 PROCEDURE  NO.
                                                      TP-801

                                                 PAGE.JLOF _ii_
                                  SECTION IV
                     |PRODUCTION
                       CONTROL
                 fa
CERTIFICAT
 BRANCH
       MANUFACT
      REPRESENT
     CERTIFICAT
       BRANCH
       ANALYZER
       OPERATOR
                      CERTIFICAT
                       BRANCH
C. Form 707-01

F. Analyzer Traces

G. Form 707-02

H. CVS Temp.  Trace

J. Preliminary Results

N. Form 707-01

Q. HWFET re-test

R. HWFET clearance

S. HWFET driver's trace

T. HWFET preliminary
   results
 Test Sequence
      401
      402
      403
                    Test Description

The Certification Branch representative receives
the preliminary FTP  results from the Data Branch,
checks it and clears for HWFET.  Production
Control initiates the HWFET.

Upon completion of the HWFET, the results are
submitted to Data Validation by the CVS operator.

The analyzer traces  are checked for errors and
the concentrations are entered onto form #707-01
(HWFET CVS).   The form is screened for obvious
errors and submitted to the Data Branch for
preliminary analysis.
                                     289
                               Data Output

-------
REVISIONS:
                                 DATA VALIDATION
                          TEST    PROCEDURE
                                                 PROCEDURE  NO.
                                                     TP-801
                                                 PAGE-JLOF
                                                                             11
 Test Sequence
      404
                   Test Description

The supporting documentation is checked off and
entered into  the FTP file for the vehicle.
          Data Output
      405       The Certification Branch representative obtains
                the HWFET preliminary results  from the Data
                Branch.  If the results are  accepted as
                valid, the representative delivers the results
                to Data Validation.

      405A      If the results are rejected, the HWFET data sheet
                is replaced and Production Control schedules a
                re-test.
                                   SECTION  V
                  V
                   j
        DATA
     VALIDATION
                            rA,C,D,E,F,H,I,J,N,S,T,U^)
                                    RODUCTION
                                    CONTROL
       DATA
    VALIDATION
                 CERTIFICATION
                    BRANCH
                   MANUFACT
                   REPRESENT
A. Form 705-01
B. Form 707-01
C. Form 705-01
E. Driver's trace
F. Analyzer traces
H. Temp. Trace,  CVS
I. Diurnal  temp.
   trace
J. Preliminary
   results
K. Official values
   (1 each)
L. Official values
   (2 each)
M. Form 707-01
   (blue copy)
N. Form 707-01
P. Form 801-01
S. HWFET driver's
   trace
T. HWFET preliminary
   results
U. Data processing
   job request
                                     290

-------
REVISIONS:
                                 DATA VALIDATION
                           TEST    PROCEDURE
PROCEDURE NO.
    TP-801

PAGE J£.OF _ii_
 Test Sequence                Test Description                  Data Output

      501       Data Validation packages all documentation and
                preliminary results from the FTP and HWFET  (if
                applicable) in file envelopes.  The complete
                file is sent  to the Data Branch for final
                processing.

      502       Following  final processing, three copies of
                the official  values print-out and the blue copy
                of form #707-01 are returned to Data Validation.

      503       Data Validation performs a final check to assure
                no obvious errors exist.  The print-outs are marked
                with the official value stamp and two copies plus
                the blue CVS  data sheet are delivered to the
                Certification Branch.  The third copy is retained
                in the vehicle file.

      504       The Certification Branch retains one copy of the
                official values and the blue copy of form #707-01
                in their file.  One copy of the official values
                is sent to the Manufacturer's Representative.

      505       The weekly activity report, form #801-01, is
                compiled and  sent to Production Control by
                4:00 p.m.  each Monday.  One copy is sent to
                Test Operations file and one is retained in the
                Data Validation file.
                                       291

-------
REVISIONS:

DATA VALIDATION
TEST PROCEDURE
PROCEDURE NO.
TP-801
PAGE n OF J£_
9.0  DATA INPUT

     9.1  This information is contained in Section 8.0.

10.0 DATA ANALYSIS

     10.1 Analysis is performed by the Data Branch using the following computer
          programs.

               o    1975 SAQF:NEWCVS-FTP

               O    SAQF:NEWCVS-HWFET

11.0 DATA OUTPUT

     11.1 This information is contained in Section 8.0.

12.0 ACCEPTANCE CRITERIA

     12.1 Acceptance criteria for data input to the Data Validation section is
          explained in previous procedures.  For acceptance limits reference
          Section 12.0 of the following procedures.

          12.1.1    Evaps - Procedure TP-705 and TP-708

          12.1.2    Prep,  and Preconditioning - Procedure TP-702 and TP-703

          12.1.3    Urban dyno test - Procedure TP-706 and TP-707

          12.1.4    HWFET - Procedure TP-710, TP-711 and TP-712

13.0 QUALITY PROVISIONS

     13.1 The Q.A. Department should audit final results to assure all entries
          and results are within acceptable limits.

     13.2 A statistical inference study should also be made of typical problems
          and solutions from data compiled in the vehicle files.  This study
          can be performed by using control charts, analysis of variance, and
          error analysis techniques.
                                     292

-------
                        F.T.P.  MINUS >WAP PLUS F.E.T.

                       DRIVER'S PRECONDITIONING REPORT
Vehicle mfgr.


No.
Time Out Time In
Date
I. VEHICLE INSPECTION
A. Valid License Plate
B. Exhaust Adaptor
C. Fuel Drain
D. Vehicle Damage

Odom




Testfl
DOK
DOK
DOK
DOK
D.None
D None
D None
DNote
F.
G.
Hi
I.
Mfgr's Data Sheet
Oil level; if low
notify Prod. Cont.
Odom Reading
Fuel level/ 1/4-
DOK
DOK
DOK

DNonc
D Note

         (note  on reverse)

     E.   Equip,  not con-
         nected notify
         Prod.  Cont.
D OK
           Note
   tank rain,;  add if
   required.

J. Start-up per Mfg. DOK
   instructions

K. Drive AMA route   DOK
II.   AMA PRECONDITIONING

     A.   Engine  Start

     B.   Ignition  Switch

     C.   Starter Motor

     D.   Fast  Idle

     E.   Transmission

     F.   Clutch

     G.   Brakes

     H.   Driveability
 Dcood          DHard

 DOK            D other

 DOK            D Grinds

 D OK            D None

 D OK            D Shifts Hard

 D OK     Grabs  D Slips

D OK     Fade   D Poor
                              D False



                              D No  Start

                              D Engine  Hot



                              D N/A

                              D' None
D Surge   Dstumble   DBack Fire  D Stretchy
  Engine Miss D       DieselsO
D OK
    Driver's  Signature
     Form 701-01
                                   293

-------
II.  SPECIFICATION CHECK                                       INITIAL
  <
     A.  Idle CO             Rt	%   Lt	%         	
     B.  Engine RPM          Idle	    Drive_

     C.  Ignition Timing     	@	inDD/ND

     D.  Fuel Drain

     E.  Wheel to driveshaft ratio
         10 wheel turns to 	driveshaft revs. N/V	

     P.  Sire size        x       .
     G.  Vehicle Weight 	with 	 tank fuel

     H.  Add 40% evap. fuel.  Witness Sig. 	
IV.  DYNAMOMETER HOT LA-4

     A.  Drive vehicle onto dyno.
         Set inertia 	Ibs. @	H.P.

     B.  Check Varian.  DPaper-OK  DPen-OK  DInk-OK  DZero-OK

     C.  Start Cooling Fan  DOK  D Release Dyno Brake-OK
                            D Tire  Pressure 45 P.S.I.-OK

     D.  Hook-up   D Chock Blocks-OK   DCable Winch   D Exhaust
                                    \
     E.  Drive to Soak Area per schedule.

     F.  11-Hour Soak Start 	  (DO NOT RE-START ENGINE
         AFTER SHUT DOWN).

     G.  DO NOT START TEST BEFORE 	AM/PM. (Add 11 hours
         to hot soak start time).
     Technician's Signature^


     Leader/Supv. Signature
                                      29k

        Form 701-01 Cont.

-------
                    VEHICLE TEST AND EVAPORATIVE DATA



Vehicle Mfgr.	No.
Inertia Wt . 'HP A/C Test »

I. HEAT -BUILD TECH
A. Drain fuel
B. Plumb air cleaner

C. Plumb canister

D. Plumb bowl vent (if required)

E. Trap gas cap (if required)

F. Seal orifices/vents
G. Install carbon traps (record on data sheet)

H. Hook-up temperature recorder

I. Hook-up thermocouple leads

J. Install heat blanket
1
K. Plug in fuel tank heater (when used)

L. Refuel vehicle - 40?0 of tank capacity
Tech. Sic- Witness Sig.
M. Replace fuel cap, plug exhaust pipe(s) Unclamp canister
Heat Build Fuel Temp. Fuel Temp. Ambient
Progress Lead No. 1 Lead No. 4 Temp.
0-Min.
15-Min.
30-Min.
45-Min.
60-Min.

II. DYNAMOMETER WARM-UP/SET
A. Drive non-test vehicle onfo dyno B. Hook-up vehicle as
C. Set inertia Ibs.Q II. P. D. Drive QSOmph steady
K. Remove vehicle trom clvno
I. Tech. Sig. Date
D
a
n

n

D

n

a
n

n

a

a

D


D









for
CTA
D
D
D

n

D

n

n
D

D

n

n

D


a









Hot LA
state




295
II. Tech. Sig. ^ Date
  FORM 705-01

-------
                                                                  form 705-01 (Cont)



111   MASS. EXHAUST EMISSION'S TEST

      A.   Check Varian   Paper-OKQ Pcn-OKQ Ink-OKQ Zcro-OKD-

      B.   Cooling fan in place   OKQ Release dyno brakc-OK  Q

      C.   Hook up     Chock blocks-OKQ  Cable winch G  Exhaust Q

      D.   Tcrnp. recorder   Connect thermocouple leads Q Start recorder  G

      E.   CVS    Check fan operation Q Bngs-OKQ Rev. Ctr. Zero  G
                 Leak check-OK G      CVS Temp-OK G
                 Cell tcmp-OK  G      Return to sample Q

      F.   Drive test  trace  G     Check tire pressure (45  PSI)  D

      G.   Remove vehicle to Soak Area  G

 IV.   HOT SOAK EVAPORATIVE EMISSION'S TEST                       TECH  CTA

      A.   Reseal orifices/vents                                   G    Q

      B.   Reconnect carbon canisters and unclamp                  ^   '-'

      C.   Reconnect temp,  recorder and thermocouple leads          Q   Q
LI. L-ilUCK gab l_cip
E. Plug exhaust pipe(s)
F. 1-hour soak Start time End

G. Start amb . temp. End amp.
H. Check ambient temp, at 15-min.
I. End of hot soak - reel amp canis
J. Shut-off temp, recorder

K. Weigh canisters and record on d

temp .
intervals
tcrs and remove


ata sheet
D
G
D
G
G
G


G
G
D
G
G
D
G


D
  V.   DE-PREP AND VEHICLE REMOVAL

      A.  'Remove  all  collection tubing,  exhaust  pipe plug(s),
          orifice/vent  plugs,  tape,  foil,  etc.                   G    Q
      B.   Disconnect  temp,  recorder  f, thermocouple leads        Q    p
      C.   Return  engine to  Mfgr's running  configuration         G    G
      D.   Move vehicle  to East lot   keys  to Prod. Contr.       p    p
      E.   "VOID"  or "FAILED" vehicles -  check with Team Leader   '
          for disposition
      F.   Leave as is,  if acceptable for I1WFET
Til.   Tech.  Sig..              	            	 Date	
 IV.   Tech.  Sig.        	 Datc_
                                       296
  V.   Tech.  Sig.	Date

-------
            EVAPORATIVE EMISSION WEIGHING  DATA
     TEST NO.
     DATE
     MAKE OF CAR
CANISTER NO.
CANISTER LOCATION
HOT SOAK WEIGHT
INITIAL WEIGHT
EVAP. EMISSIONS





f i














     TOTAL EVAP. EMISSIONS
FORM 705-02
                              297

-------
                                  CONSTANT VOLUME SAMPLER (CVS) DATA  SHEET
o
3
O
1
o
M
UANF.
CODE




MODEL
-




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REQUESTED
	 DATE 	


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15
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STROKE

FU


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VEHICLE




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IGN.
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RcCLESTC^ COMV'tNTS




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G I I RPM | %CO
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is



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CURB NO.
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TEST NO.

         LABORATORY COMMENTS
                                                                                 (- cvs HOURS —[  |  | ITEST NO.
                                                                                 111i i iTIoul rmtn
I r
ro
BA
BA
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-------
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                                     299
      form 707-02

-------
                                                                 Form  801-01
                         ENVIRONMENTAL PROTECTION AGENCY


                       Ann  Arbor, Michigan 48105


Light Duty Testing Schedule for	
                                          Date
                                          Submitted
  E-
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-------
Submitted by:
Project number:
   IN
DATE:

TIME:
Application name:

Number of runs:
                                                               TP-801
                                                               Attachment No.  1
                            DATA PROCESSING JOB REQUEST
                                                        Job  No. 01569
Additional copies of results:
                             Branch:
Section:
                                                    DATE:
                                                    TIME:
                                                    Completed by:
                                        Results needed by:

                                        Urgency: 	
Data processing section use

Program modifications:	
Special  I/O  requirements:

Pre-run preparation:	
                                 Program  name(s):
                                                Computer usage:  CCU

                                                               CLT
NAPCA (DUR) 165
      7/70
                                                                    job  NO.  01569
                                       301

-------
900

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                        Section 900
            PROGRAM PLANNING AND QUALITY AUDIT
Currently no procedures are included in this Section of
the manual.  Those procedures pertaining to this Section
must be supplied by the user and may be supplied by the
EPA in subsequent revisions.
                             303

-------
                                    TECHNICAL REPORT DATA
                             (Please read Instructions on the reverse before completing)
1. REPORT NO.
EPA-650/4-75-024-b
             3. RECIPIENT'S ACCESSION-NO.
4. TITLE AND SUBTITLE
 uidelines for QA Programs  for Mobile Source  Emissions
Measurement Systems -  Phase I, Light Duty  Gasoline-
Powered Vehicles - Test  Procedures
             5. REPORT DATE
               June 1975
             6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S)
Rod  Pilkington, Tom Kelly and Harold Wimette
             8. PERFORMING ORGANIZATION REPORT NO,
9. PERFORMING ORGANIZATION NAME AND ADDRESS
Olson Laboratories, Inc.
421  East Cerr.itos Avenue
Anaheim, California   92805
             10. PROGRAM ELEMENT NO.
               1HA327
             11. CONTRACT/GRANT NO.
               68-02-1740
 12. SPONSORING AGENCY NAME AND ADDRESS
 EPA,  NERC, QAEML, QAS
 Research Triangle Park
 North Carolina  27711
             13. TYPE OF REPORT AND PERIOD COVERED
               Final
             14. SPONSORING AGENCY CODE
 15. SUPPLEMENTARY NOTES This  report is one of  two  volumes for Light Duty  Gasoline-Powered
 Vehicles (Phase I).  Other volumes are to  be issued for Phase II Heavy Duty Diesel
 Engines, Phase III Light  Duty Diesel-Powered Vehicles, and Phase IV Heavy Duty Gasoline
Test  Procedures for Light Duty Gasoline-Powered Mobile Source Emissions  Measurement
Systems are presented with the concept of  a  total Quality Assurance  System.   The
Test  Procedures are presented in document  control format and give  the  detailed
test  procedures with Quality Assurance provisions for each part of the total
testing _system>
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                               b.lDENTIFIERS/OPEN ENDED TERMS
                                                Mobile Source Emission
                                                Testing
                             COSATl Field/Group
                            T3TT
                             14D
                             07D
                             13B
Quality Control
Quality Assurance
Quantitative Analysis
Gas Analysis
Emissions  -  Exhaust Gases
Compliance Testing
Air Pollution
18. DISTRIBUTION STATEMENT
Unlimited
19. SECURITY CLASS (This Report)
 Unclassified      	
                                                                          21. NO. OF PAGES
                                                                            316	
                                               20. SECURITY CLASS (This page)
                                                                          22. PRICE
EPA Form 2220-1 (9-73)

-------
                                                         INSTRUCTIONS

    1.   REPORT NUMBER
        Insert the EPA report number as it appears on the cover of the publication.

    2.   LEAVE BLANK

    3.   RECIPIENTS ACCESSION NUMBER
        Reserved for use by each report recipient.

    4.   TITLE AND SUBTITLE
        Title should indicate clearly and briefly the subject coverage of the report, and be displayed prominently.  Set subtitle, if used, in smaller
        type or otherwise subordinate it to main title. When a report is prepared in more than one volume, repeat the primary title, add volume
        number and include subtitle for the specific title.

    5.   REPORT DATE
        Each report shall carry a date indicating at least month and year.  Indicate the basis on which it was selected (e.g., date of issue, date of
        approve/, date of preparation, etc.).

    6.   PERFORMING ORGANIZATION CODE
        Leave blank.

    7.   AUTHOR(S)
        Give name(s) in conventional order (John R. Doe, J. Robert Doe, etc.). List author's affiliation if it differs from the performing organi-
        zation.

    8.   PERFORMING ORGANIZATION REPORT NUMBER
        Insert if performing organization wishes to assign this number.

    9.   PERFORMING ORGANIZATION NAME AND ADDRESS
        Give name, street, city, state, and ZIP code.  List no more than two levels of an organizational hirearchy.

    10. PROGRAM ELEMENT NUMBER
        Use the program element number under which the report was prepared. Subordinate numbers may be included in parentheses.

    11. CONTRACT/GRANT NUMBER
        Insert contract or grant number under which report was prepared.

    12. SPONSORING AGENCY NAME AND ADDRESS
        Include ZIP code.

    13. TYPE OF REPORT AND PERIOD COVERED
        Indicate interim final, etc., and if applicable, dates covered.

    14. SPONSORING AGENCY CODE
        Leave blank.

    15. SUPPLEMENTARY NOTES
        Enter information not included elsewhere but useful, such as:  Prepared in cooperation with. Translation of, Presented at conference of,
        To be published in, Supersedes, Supplements, etc.

    16. ABSTRACT
        Include a brief (200 words or less) factual summary of the most significant information contained in the report. If the report contains a
        significant bibliography or literature survey, mention it here.

    17. KEY WORDS AND DOCUMENT ANALYSIS
        (a) DESCRIPTORS - Select from the Thesaurus of Engineering and Scientific Terms the proper authorized terms that identify the major
        concept of the research and are sufficiently speciflc.and precise to be used as index entries for cataloging.

        (b) IDENTIFIERS AND OPEN-ENDED TERMS - Use identifiers for project names, code names, equipment designators, etc.  Use open-
        ended terms written in descriptor form for those subjects for which no descriptor exists.

        (c) COSATI FIELD GROUP - Field and group assignments are to be taken from the 1965 COSATI Subject Category List Since the ma-
        jority of documents are multidisciplinary in nature, the Primary Field/Group assignment(s) will be specific discipline, area of human
        endeavor, or type of physical  object.  The application(s) will be cross-referenced with secondary Field/Group assignments that will follow
        the primary posting(s).

    18. DISTRIBUTION STATEMENT
        Denote reusability to the public or limitation for reasons other  than security for example "Release Unlimited."  Cite any availability to
        the public, with address and price.

    19.8.20.  SECURITY CLASSIFICATION
        DO NOT submit classified reports to the National Technical Information service.

    21. NUMBER OF PAGES
        Insert the total number of pages, including this one and unnumbered pages, but exclude distribution list, if any.

    22. PRICE
        Insert the price set by the National Technical Information Service or the Government Printing Office, if known.
EPA Form 2220-1 (9-73) (Reverse)

-------