United States
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park, NC 27711
EPA-454/R-99-024C
August 1999
AIR
SEPA
Air Emissions From
Reinforced Plastics Composite
Manufacturing Process
LASCO Panel Products: Volume
-------
FINAL REPORT
AIR EMISSIONS FROM
REINFORCED PLASTICS COMPOSITE
MANUFACTURING PROCESS
LASCO PANEL PRODUCTS
VOLUME III OF III
APPENDICES B THROUGH E
EPA Contract No. 68D70069
Work Assignment No. 2-10
Prepared for:
Mr. Solomon Ricks (MD-19)
Work Assignment Manager
SMTG, EMC, EMAD, OAQPS
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
August 1999
P:\i530\finrpt
Submitted by
PACIFIC ENVIRONMENTAL SERVICES, INC.
5001 South Miami Blvd., Suite 300
PO Box 12077
Research Triangle Park, NC 27709
(919)941-0333
Fax: (919)941-0234
-------
DISCLAIMER
This document was prepared by Pacific Environmental Services, Inc. (PES) under
EPA Contract No. 68D70069, Work Assignment No. 2-10. This document has passed
PES' internal quality assurance review and has been approved for distribution. The
contents of this document do not necessarily reflect the views and policies of the U.S.
EPA. Mention of trade names does not constitute endorsement by the EPA or PES.
11
-------
TABLE OF CONTENTS
VOLUME I Page
1.0 INTRODUCTION 1-1
2.0 SUMMARY OF TEST RESULTS 2-1
2.1 EMISSIONS TEST LOG 2-1
2.2 PROCESS LINE RESULTS 2-4
2.3 TOTAL TEMPORARY ENCLOSURE - METHOD 25A
TOTAL HYDROCARBON RESULTS 2-5
2.4 TOTAL TEMPORARY ENCLOSURE - VOLUMETRIC AIR
FLOW RATE RESULTS 2-5
2.5 TOTAL TEMPORARY ENCLOSURE - METHOD 18 RESULTS .. 2-5
2.6 OVEN NOS. 9 AND 10 - METHOD 25A TOTAL
HYDROCARBON RESULTS 2-23
2.7 OVEN NOS. 9 AND 10 - VOLUMETRIC FLOW RATE
RESULTS 2-23
2.8 OVEN NOS. 9 AND 10 - METHOD 18 HAP RESULTS 2-23
2.9 UNCATALYZED RESIN (UCR) AND GEL COAT
SAMPLE RESULTS 2-23
2.10 RESPONSE FACTOR RESULTS 2-41
2.11 METHOD 204 TOTAL TEMPORARY ENCLOSURE
VERIFICATION 2-41
3.0 PROCESS DESCRIPTION 3-1
4.0 SAMPLING LOCATIONS 4-1
4.1 MAIN EXHAUST STACK 4-1
4.2 ROOM EXHAUST STACK 4-1
4.3 AUXILIARY EXHAUST STACK 4-4
4.4 NATURAL DRAFT OPENINGS 4-4
4.5 OVEN EXHAUST NO. 9 AND NO. 10 4-4
in
-------
TABLE OF CONTENTS (Continued)
5.0 SAMPLING AND ANALYTICAL PROCEDURES 5-1
5.1 LOCATION OF MEASUREMENT SAMPLE/VELOCITY
TRAVERSE POINTS 5-1
5.2 DETERMINATION OF STACK GAS VOLUMETRIC
FLOW RATE 5-1
5.3 DETERMINATION OF DRY MOLECULAR WEIGHT 5-4
5.4 EXHAUST GAS MOISTURE CONTENT 5-4
5.5 DETERMINATION OF HAZARDOUS AIR POLLUTANTS 5-4
5.6 DETERMINATION OF TOTAL HYDROCARBONS 5-6
5.7 DETERMINATION OF VOLATILE MATTER CONTENT,
DENSITY, VOLUME OF SOLIDS, WEIGHT OF SOLIDS,
WATER CONTENT, AND HAPS BY DISTILLATION 5-6
5.8 RESPONSE FACTORS FOR FLAME IONIZATION
ANALYZERS 5-10
6.0 QUALITY ASSURANCE/QUALITY CONTROL 6-1
6.1 CALIBRATION OF APPARATUS ... > 6-1
6.2 ONSITE QA/QC 6-3
APPENDIX A - RAW FIELD DATA
Appendix A. 1 Manual Methods Raw Field Data
A. 1.1 Method 1 Field Data Sheets (includes flows, moistures, and
Method 18)
A. 1.2 Condition 1 (includes flows, moistures, and Method 18)
A. 1.3 Condition 2 (includes flows, moistures, and Method 18)
A. 1.4 Condition 3 (includes flows, moistures, and Method 18)
A. 1.5 Condition 4 (includes flows, moistures, and Method 18)
A. 1.6 Condition 5 (includes flows, moistures, and Method 18)
A. 1.7 Condition 6 (includes flows, moistures, and Method 18)
A. 1.8 Condition 7 (includes flows, moistures, and Method 18)
A. 1.9 Condition 8 (includes flows, moistures, and Method 18)
A. 1.10 Condition 9 (includes flows, moistures, and Method 18)
A. 1.11 Condition 10 (includes flows, moistures, and Method 18)
A. 1.12 Condition 11 (includes flows, moistures, and Method 18)
A. 1.13 Condition 12 (includes flows, moistures, and Method 18)
A. 1.14 Condition 13 (includes flows, moistures, and Method 18)
A. 1.15 NDO Summary Data
iv
-------
TABLE OF CONTENTS (Continued)
VOLUME II
Appendix A.2 Instrumental Methods Raw Field Data
A.2.1 TTE Static Pressures
A.2.2 Method 25A Calibration Data
A.2.3 Condition 1 Method 25A
A.2.4 Condition 2 Method 25A
A.2.5 Condition 3 Method 25A
A.2.6 Condition 4 Method 25A
A.2.7 Condition 5 Method 25A
A.2.8 Condition 6 Method 25A
A.2.9 Condition 7 Method 25A
A.2.10 Condition 8 Method 25A
A.2.11 Condition 9 and 10 Method 25A
A.2.12 Condition 11 Method 25A
A.2.13 Condition 12 Method 25A
A.2.14 Condition 13 Method 25A
A.2.15 Conditions 1-13 Method 25A Strip Charts
A.2.16 OvenNos. 9 and 10 Method 25A
VOLUME III
APPENDIX B - ANALYTICAL DATA
B. 1 Method 18 Analytical Data
B.2 Method 18 GC Chromatograms
APPENDIX C - CALCULATIONS
APPENDIX D - QA/QC DATA
APPENDIX E - PROJECT PARTICIPANTS
-------
LIST OF TABLES
VOLUME I
Table 1.1 LASCO Panel Products Test Matrix 1-6
Table 2.1 Emission Test Log, LASCO Panel Products, Florence, Kentucky 2-2
Table 2.2 TTE Total Hydrocarbon Mass Emission Rate Summary 2-6
Table 2.3 Summary of TTE Stack Gas Conditions, and THC Concentrations
and Mass Emission Rates, Condition 1 - May 14,1997 2-8
Table 2.4 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 2 - May 14,1997 2-9
Table 2.5 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 3 - May 15,1997 2-10
Table 2.6 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition4 - May 15,1997 2-11
Table 2.7 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 5 - May 19,1997 2-12
Table 2.8 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 6 - May 19,1997 2-13
Table 2.9 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 7 - May 20,1997 2-14
Table 2.10 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 8 - May 22, 1997 2-15
Table 2.11 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 9 - May 22, 1997 2-16
Table 2.12 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 10 - May 22, 1997 2-17
Table 2.13 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 11 - May 23,1997 2-18
Table 2.14 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 12 - May 29,1997 2-19
Table 2.15 Summary of TTE Stack Gas Conditions and THC Concentrations -
Condition 13 - May 29,1997 2-20.
Table 2.16 TTE Mass Rate Summary - Styrene, Methyl Methacrylate, and
Cumene by EPA Method 18 2-21
Table 2.17 Ovens 9 and 10 THC Mass Emission Rate Summary 2-24
VI
-------
LIST OF TABLES (Concluded)
Table 2.18 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 1 - May 14,1997 2-26
Table 2.19 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 2 - May 14,1997 2-27
Table 2.20 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 3 - May 15,1997 2-28
Table 2.21 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 4 - May 15,1997 2-29
Table 2.22 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 5 - May 19,1997 2-30
Table 2.23 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 6 - May 19, 1997 2-31
Table 2.24 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 7 - May 20,1997 2-32
Table 2.25 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 8 - May 22,1997 2-33
Table 2.26 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 9 - May 22,1997 2-34
Table 2.27 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 10 - May 22, 1997 2-35
Table 2.28 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 11 - May 23,1997 2-36
Table 2.29 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 12 - May 29,1997 2-37
Table 2.30 Summary of Oven Stack Gas Conditions and THC Concentrations
and Mass Emission Rates, Condition 13 - May 29,1997 2-38
Table 2.31 Ovens 9 and 10 Mass Emission Rate Summary - Styrene,
Methyl Methacrylate, and Cumene by EPA Method 18 2-39
Table 2.32 Summary of Response Factor Results - Styrene Bag Standards 2-42
Table 5.1 Sources, Test Parameters, and Methods Summary
LASCO Panel Products - Florence, Kentucky 5-2
Table 6.1 Summary of Temperature Sensors Calibration Requirements 6-2
Table 6.2 Summary of Calibration Results for THC Analyzers
Condition Nos. 1-13, LASCO Panel Products 6-5
Table 6.3 Summary of EPA Method 18 Quality Assurance Results
Styrene Recovery Efficiencies 6-7
Table 6.4 Summary of Desorption Efficiencies 6-7
vn
-------
LIST OF FIGURES
VOLUME I Page
Figure 1.1 Key Personnel and Responsibility for Testing at LASCO
Panel Products 1-2
Figure 1.2 Overview of Sampling Locations 1-5
Figure 2.1 Diagram of Temporary Total Enclosure 2-43
Figure 4.1 Main Exhaust Sample Location 4-2
Figure 4.2 Room Exhaust Sample Location 4-3
Figure 4.3 Auxiliary Exhaust Sampling Location 4-5
Figure 4.4 Natural Draft Opening Sampling Location 4-6
Figure 4.5 Oven No. 9 Schematic of Sampling Location 4-7
Figure 4.6 Oven No. 10 Schematic of Sampling Location 4-8
Figure 5.1 Schematic of EPA Method 4 Sampling Train 5-5
Figure 5.2 Schematic of EPA Method 18 Sampling System -
Sorbent Tube Method 5-7
Figure 5.3 Schematic of Methane/Ethane Sampling System 5-8
Figure 5.4 EPA Method 25A Total Gaseous Organic Analyzer and
Sample System 5-9
Figure 5.5 Schematic of Bag Standard Preparation System 5-13
vni
-------
APPENDIX B
ANALYTICAL DATA
-------
APPENDIX B.I
Method 18 Analytical Data
-------
Gary, NC 27519
1-800-733-3261 Fax (919) 250-1835
July 29, 1997
Mr. Dan Scheffel
Pacific Environmental Services, Inc
4700 Duke Drive, Suite 150
Mason, Ohio 45040
Dear Mr. Sheffel,
Enclosed with this letter are printouts and an electronic copy of the GC data from the
PES/EPA task performed at Lasco in Florence, KY. You had requested various sets of data
deemed missing from our previous submittal. These printouts show the referenced data for
methane, ethane, styrene, cumene, and methyl methacrylate. These sheets also include
separate spike recovery results and cylinder analysis results. These are listed on separate pages
for weeks 2 and 3 to prevent confusion with sample data. Please note that values that are at or
near the calculated detection limit are flagged with a "DL", and the precision between the
duplicate injections are not calculated. The precision requirements are not applicable at the
detection limit, since by definition the detection limit is a point where the precision and
accuracy of measurements begin to vary statistically. A diskette is also included with this data
presented in a Excel format. If you have any questions, please feel free to call and discuss
these results with either myself or Pete Zemek.
Sincerely,
enclosures
-------
LASCO
Job No. 97-3020
Analyte (mg)
Tube Samples Standard Curve from 5/14/97
File:N:Y-\Lasco\97-3020\Styrene.WQ2
Low Standard
Mid Standard
High Standard
Styrene
Purity
Density
Slope
Irrtcp
AvgRF
Blank Avg
Concal
5/14/97
@ 18:44
Concal
5/14/97
@ 23:30
Concal
5/15/97
@ 12:08
Con Cal
5/15/97
@ 20:56
99.0%
0.91
234910.5
1116.1
4.14E-06
0
Styrene
Styrene
Styrene
Styrene
Inj. Vol.
Std./Fil
Peak Areas
Avg./Dev.
RF
Note: Average area
Inject 1
361653
380417
-
384658
391349
1.2
0.4
94290
94366
3.82E-06
uL
10.2%
94442
0.1%
6.0
1.8
406416
411115
4.38E-06
uL
-3.1%
415814
1.1%
12.0
3.6
848540
853400
4.22E-06
uL
0.7%
858260
0.6%
counts are reagent blank corrected
Inject 2
368725
352150
381343
374306
Average
365189
366284
383001
382828
Deviation
1.0%
3.9%
0.4%
2.2%
Mass (mg)
1.550
1.6
1.6
1.6
Expected
(mg)
1.5
1.5
1.5
1.5
Error
3.2%
3.5%
8.3%
8.2%
Blank
-------
Desorption Efficiency Study; Charcoal
Spike Level
0
0.9009
4.5045
9.009
Inject 1 Inject 2
100 < 100
185442 176639
1048067 903904
1946652 1867256
Average Deviation Mass (mg)
100 0.0% -0 00
181041 2.4% 0.77
7.4% 4,15
975986
1906954
2.1% 8.11
Average
Desorp.
Efficiency
(blank con".)
85.0%
92.1%
90.1%
89.1%
-------
Tubes
Unspiked Gas Vol.
Unspiked Gas Vol.
&-2-1A-FH Front
9-2-1A-BH Back
9-2-1B-FH 1st Back
Inject 1 Inject 2
e
e
e
14.3 dsl
6094
100 <
100 <
6266
100
100
Sample
Cone.
Average Deviation Mass (mg) (mg/cuM)
6180
100
100
1.4%
0.0%
0.0%
0.02
-0.00
-0.00
1.5
-0.3
-0.3
Unpiked Sample;
Unspl
10-1-;
-------
Unspiked Sample; M D 6 " I -"*> fTS
Gas Vol. 15.7 dsl
NDlb-1-3A- Front e 1337 1330
NDA-1-3A- Back < e 100 < 100
NDf-1-3A- 1st Back < e 100 < 100
1334
100
100
0.3%
0.0%
0.0%
0.00
-0.00
-0.00
0.1
-0.3
-0.3
Unspiked Sample; MB -1 - 3 pf *>
Gas Vol. 6.2 dsl
ME-1-1A-F Front E e 3934626 E
ME-1-fA-B Back < e 100 <
ME-1-/B-F 1st Back < e 100 <
Unspiked Sample;
Gas Vol. 8.9 dsl
ME-2-1A-F Front E e
ME-2-1A-B Back < e
ME-2-1B-F 1st Back < e
3894949
100
100
4394997 E 4322457
100 < 100
100 < 100
3914788
100
100
4358727
100
100
0.5%
0.0%
0.0%
0.8%
0.0%
0.0%
16.66
-0.00
-0.00
18.55
-0.00
-0.00
2682.8
-0.7
-0.7
2084.3
-0.5
-0.5
Unspiked Sample;
Gas Vol. 8.8 dsl
ME-2-1B-F Front e
ME-2-1B-B Back < e
ME-2-1B-F 1st Back < e
Spiked Sample;
Gas Vol. 2.3 dsl
ME-3-3A-F Front e
ME-3-3A-B Back < e
ME-3-3B-F 1st Back < e
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Actual Spiked Mass (mg)
UNSpiked Sample;
Gas Vol. 2.3 dsl
ME-3-3A-F Front e
ME-3-3A-B Back < e
ME-3-3B-F 1st Back < e
Spike Recovery %
% of Theoretical
100 <
100 <
100
100
0
100
100
ERR
0.0%
0.0%
-0.00
-0.00
-0.00
-0.8
-0.5
-0.5
742801
100 <
100 <
2.5
2.53
2.56
782920
100
100
762861
100
100
2.6%
0.0%
0.0%
3.24
-0.00
-0.00
1441.2
-1.9
-1.9
158837
100 <
100 <
101.3%
371.9%
162860
100
100
160849
100
100
1.3%
0.0%
0.0%
0.68
-0.00
-0.00
302.2
-1.9
-1.9
-------
Unspiked Sample; -1 -3
Gas Vol. 14.6 dsl
RE-1-1A-F Front e 729930
RE-1-IA-B Back e 1106
RE-1-fB-F 1st Back < e 100 <
Unspiked Sample;
Gas Vol. 14.7 dsl
RE-2-1A-F Front e
RE-2-1A-B Back < e
RE-2-1B-F 1st Back < e
Spiked Sample;
Gas Vol. 2.3 dsl
RE-4-1A-F Front e
RE-4-1A-B Back < e
RE-4-1B-F 1st Back < e
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Actual Spiked Mass (mg)
Unspiked Sample;
Gas Vol. 2.3 dsl
RE-4-1A-F Front e
RE-4-1A-B Back < e
RE-4-1B-F 1st Back < e
Spike Recovery %
% of Theoretical
1230510
100 <
100 <
121917
100
100
0.25
0,35
0.44
745980
808
100
1168310
100
100
125805
100
100
737955
957
100
1199410
100
100
123861
100
100
1.1%
15.6%
0.0%
2.6%
0.0%
0.0%
1.6%
0.0%
0.0%
3.-14
-000
-0.00
5.10
-0.00
-0.00
0.52
-0.00
-0.00
214.8
-0.0
-0.3
346.8
-0.3
-0.3
2322
-1.9
-1.9
19431
100 <
100 <
127.1%
449.8%
19358
100
100
19395
100
100
0.2%
0.0%
0.0%
0.08
-0.00
-0.00
5.3
-1.9
•1.9
-------
LASCO
Job No. 97-3020
Analyte (mg)
Tube Samples
File:N:V-\Lasco\97-3020\Cumene.WQ2
Low Standard Mid Standard
Standard Curve from 5/14/97
High Standard
Cumene
Purity
Density
Slope
Irrtcp
AvgRF
Blank Avg
Concal
5/14/97
@ 18:44
Concal
5/14/97
@ 23:30
Concal
5/15/17
@ 12:08
Concal
5/15/97
©20:58
99.9%
0.88
228592.9
-10752.8
4.64E-06
0
Cumene
Cumene
Cumene
Cumene
Inj. Vol.
Std./Fit
Peak Areas
Avg./Dev.
RF
Note: Average area
Inject 1
311554
327082
.-
330319
336637
1.5
0.4
93703
91288.5
4.71 E-06
uL
3.9%
88874
2.6%
6.0
1.7
350253
353743.5
4.86E-06
uL
-7.2%
357234
1.0%
12.0
3.4
785786
788386
4.36E-06
uL
1.7%
790985
0.3%
counts are reagent blank corrected
Inject 2
316622
301611
329017
323555
Average
314088
314347
329668
330096
Deviation
0.8%
4.1%
0.2%
2.0%
Mass (mg)
1.4
1.4
1.5
1.5
Expected
(mg)
1.4
1.4
1.4
1.4
Error
-0.7%
-0.7%
4.0%
4.1%
-------
Desorption Efficiency Study; Charcoal
Inject 1
Spike Level
(mg)
0
0.86
4.3
8.6
Inject 2
100 < 100
267850 253391
1413161 1214978
2418484
2317357
2859174
Average Deviation Mass (mg)
16 900.0% 0.05
260621 2.8% 1.19
1314070 7.5% 5.80
2367921 2.1% 10.41
Average
Desorp.
Efficiency
(blank coir.)
138.0%
134.8%
121.0%
131.3%
-------
Tubes
i Sample
i Cone.
Unpiked Sample; Inject 1 Inject 2 Average Deviation Mass(mg) (mg/cuM)
Unspiked Gas Vol. 14.3 dsl
9-2-1A-FH Front < e 100 < 100 100 0.0% 0.05 3,3
0-2-1 A-BH Back < e 100 < 100 100 0.0% 0.05 3.3
&-2-1B-FH 1st Back < e 100 < 100 100 0.0% 0.05 3.3
Unpiked Sample;
Unspiked Gas Vol. 15.5 dsl
10-1A-FH Front < e 100 < 100 100 0.0% 0.05 3.1
10-1A-BH Back < e 100 < 100 100 0.0% 0.05 3.1
10-1B-FH 1st Back < t 100 < 100 100 0.0% 0.05 3.1
Unpiked Sample; Ib-l-l
Unspiked Gas Vol. 15.5 dsl
10-1-tA-FH Front < e 100 < 100 100 0.0% 0.05 3.1
10-1-aA-BH Back < e 100 < 100 100 0.0% 0.05 3.1
1Q-1-2B-FH 1st Back < e 100 < 100 100 0.0% 0.05 3.1
-------
Unspiked Sample;
Gas Vol. 14.6 dsl
NDA-HA-FH Front <
NDA-1A-BH Back <
NDA-1B-FH 1st Back <
Unspiked Sample;
Gas Vol. 14.6 dsl
NDA-2-2A- Front <
NDA-2-2A- Back <
NDA-2-2B- 1st Back <
100 <
100 <
100 <
100
100
100
100
100
100
0.0%
0.0%
0.0%
0.05
0.05
0.05
3.3
3.3
3.3
e
e
e
100 <
100 <
100 <
100
100
100
100
100
100
0.0%
0.0%
0.0%
0.05
0.05
0.05
3.3
3.3
3.3
Unspiked Sample;
Gas Vol. 14.6 dsl
NDB-2-3A- Front < e 100 < 100
NDB-2-3A- Back < e 100 < 100
NDB-2-3B- 1st Back < e 100 < 100
100
100
100
0.0%
0.0%
0.0%
0.05
o.os
0.05
3.3
3.3
3.3
Unspiked Sample; NDK»-l-3 PT5
Gas Vol. 15.7 dsl
NDlb-1-3A- Front < e 100 < 100
NDB-1-3A- Back < e 100 < 100
NDIp-1-3B- 1st Back < e 100 < 100
100
100
100
0.0%
0.0%
0.0%
0.05
0.05
0.05
3.0
3.0
3.0
Unspiked Sample; M£-l~"2>
Gas Vol. 6.2 dsl
ME-1-fA-F Front e
ME-14A-B Back < e
ME-1-fB-F ist Back < e
Unspiked Sample;
3216
100 <
100 <
3286
100
100
3251
100
100
1.1%
0.0%
0.0%
0.06
0.05
0.05
9.9
7.6
7.6
Gas Vol. 8.9 dsl
ME-2-1A-F Front
ME-2-1A-B Back <
ME-2-1B-F 1st Back <
e
e
e
5050
100 <
100 <
4920
100
100
4985
100
100
1.3%
0.0%
0.0%
0.07
0.05
0.05
7.8
5.4
5.4
-------
Unspiked Sample;
Gas Vol. 8.9
ME-2-1B-F Front
ME-2-1B-B Back
ME-2-1B-F 1st Back
Unspiked Sample;
e
e
e
100
100
100
100
100
100
100
100
100
ERR
0.0%
0.0%
0.05
0.05
0.05
5.4
5.4
Gas Vol.
ME-3-3A-F
ME-3-3A-B
ME-3-3B-F
2.5
Front
Back
1st Back
dsl
<
<
e
e
e
1072
100
100
<
<
1128
100
100
1100
100
100
2.5%
0.0%
0.0%
0
0
0
.05
.05
.05
20.7
19.0
18.0
7/it
Unspiked Sample;
Gas Vol. 14.6 dsl
RE-1-U-F Front < e
RE-1-IA-B Back < e
RE-1-IB-F 1st Back < e
Unspiked Sample;
Gas Vol. 14.7 dsl
RE-2-1A-F Front < e
RE-2-1A-B Back < e
RE-2-1B-F 1st Back < e
Unspiked Sample;
Gas Vol. 14.7 dsl
RE-4-1A-F Front < e
RE-4-1A-B Back < e
RE-4-1B-F 1st Back < e
1187
100 <
100 <
2259
100
100
100
100
100
1136
100
100
1864
100
100
100
100
100
1162
100
100
2062
100
100
100
100
100
2.2%
0.0%
0.0%
9.6%
0.0%
0,0%
0.0%
0.0%
0.0%
0.05
0.05
0.05
0.06
0.05
0.05
0.05
0.05
0.05
3.i
3.3
3.3
„ „
3.8
3.2
3.2
3.2
3.2
3.2
-------
LASCO
Job No 97-3020
Analyte (mg)
Methyl Methacrylate
Tube Samples Standard Curve from 5/14/97
File: N:\--\Lasco\97-3020\MMA.WQ2
Low Standard
Mid Standard
High Standard
Purity
Density
Slope
Intcp
AvgRF
Blank Avg
Concal
5/14/97
@ 18:44
Concal
5/14/97
@ 23:30
Concal
5/15/97
@ 12:08
Concal
5/15/97
@ 20:56
99.0%
0.94
117474.6
-3657.0
8.69E-06
Inj. Vol.
Std./Fit
Peak Areas
AvgVDev.
RF
0 Note: Average area
Methyl Methaciyl
Methyl Methacryl
-
Methyl Methacryl
Methyl Methacryl
Inject 1
169927
176763
177144
177854
1.2
0.4
45804
44957
8.28E-06
~uL
11.2%
44110
1.9%
6.0
1.9
201927
198876
9.36E-06
uL
-7.4%
195825
1.5%
12.0
3.7
440469
441192
8.44E-06
uL
1.7%
441914
0.2%
counts are reagent blank corrected
Inject 2
171239
162612
173999
170309
Average
170583
169688
175572
174082
Deviation
0.4%
4.2%
0.9%
2.2%
Mass (mg)
1.5
1-5
1.5
1.5
Expected
(mg)
1.6
1.6
1.6
1.6
Error
-4.4%
-4.9%
-1.6%
-2.4%
-------
Desorption Effia'ency Study; Charcoal
i
Spike Level
(mo)
0 <
0.0306
4.653
9.306
Inject 1
100 <
64370
540734
940651
Inject 2
100
61140
478995
914954
Average
100
62755
509865
927803
Deviation
0.0%
2.6%
6.1%
1.4%
Mass (mg)
0.03
0.57
4.37
7.93
Average
Oesorp.
Efficiency
(blank corr.)
60.7%
93.9%
85.2%
80.0%
-------
Tubes
Unpiked Sample;
Unspiked Gas Vol.
9-2-1A-FH Front e
9-2-1A-BH Back < e
&-2-1B-FH 1st Back < e
Inject 1
Inject 2
Average Deviation Mass (mg)
Sample
Cone.
(mg/cuM)
14.3 dsl
834
100 <
100 <
847
100
100
841
100
100
0,8% ;
0.058^
0.0%
0.04
0.03
0.03
2.7
2.2
2.2
Unspiked Gas Vol.
10-1A-FH Front e
10-1A-BH Back < e
10-1B-FH 1st Back < e
15.5 dsl
321
100 <
100 <
362
100
100
342
100
100
6.0%
0.0%
0.0%
0.03
0.03
0.03
2.2
2.1
2.1
Unpiked Sample; ID- \- { H"5
Unspiked Gas Vol.
10-1-fcA-FH Front
10-1-|A-BH Back
10-1-fB-FH 1st Back <
Unspiked Sample;
Gas Vol. 14.6 dsi
NDA-1A-FH Front e 337 332
NDA-1A-BH Back < e 100 < 100
NDA-1A-FH 1st Back < e 100 < 100
Unspiked Sample;
Gas Vol. 14.6 dsl
NDA-2-2A-F Front e 1317 1672
NDA-2-2A-B Back < e 100 < 100
NDA-2-2B-F 1st Back < e 100 < 100
e
e
e
15.5 dsl
100 <
100 <
100 <
100
100
too
100
100
100
0.0%
0.0%
0.0%
0.03
0.03
0.03
2.1
2.1
2.1
335
100
100
1495
100
100
0.7%
0.0%
0.0%
11.9%
0.0%
0.0%
0.03
0.03
0.03
0.04
0.03
0.03
2.3
2.2
2.2
3.0
2.2
2.2
Unspiked Sample;
Gas Vol. 14.7 dsl
NDB-2-3A-F Front < e 100 < 100
NDB-2-3A-B Back < e 100 < 100
NDB-2-3B-F 1st Back < e 100 < 100
100
100
100
0.0%
0.0%
0.0%
0.03
0.03
0.03
2.2
2.2
2.2
-------
Unspiked Sample;
Gas Vol. 15.7 dsl
ND»-1-3A-F Front < e
NDB-1-3A-B Back < e
NDD-1-3A-F 1st Back < e
Pr*
100 <
100 <
100 <
100
100
100
100
100
100
0.0%
0.0%
0.0%
0.03
0.03
0.03
2.0
2.0
2.0
Unspiked Sample; H£-l-"2»
Gas Vol. 6.2 dsl
ME-1-^A-FH Front e
ME-1-1A-BH Back < e
ME-1-fB-FH 1st Back < e
Unspiked Sample;
Gas Vol. 8.9 dsl
ME-2-1A-FH Front e
ME-2-1A-BH Back < e
ME-2-1B-FH 1st Back < e
rrs
591876
100 <
100 <
826657
100 <
100 <
579782
100
100
773904
100
100
585829
100
100
800281
100
100
1.0%
0.0%
0.0%
3.3%
0.0%
0.0%
5.02
0.03
0.03
6.84
0.03
0.03
808.0
5.2
5.2
771.5
3.6
3.6
Unspiked Sample;
Gas Vol. 8.9 dsl
ME-2-1B-FH Front < e
ME-2-1B-BH Back < e
ME-2-1B-FH 1st Back < e
Unspiked Sample;
Gas Vol. 2.5 dsl
ME-3-3A-FH Front e
ME-3-3A-BH Back < e
ME-3-3B-FH 1st Back < e
100 *
100 <
100 <
too
100
100
100
100
100
ERR
0.0%
0.0%
0.03
0.03
0.03
3.6
3.6
3.6
499
100 <
100 <
523
100
100
511
100
100
2.3%
0.0%
0.0%
0.04
0.03
0.03
14.2
12.8
12.8
7/28
Unspiked Sample;
Gas Vol. 14.6 dsl
-------
RE-1-tA-FH Front e 144936 146550 145743 0.6% 1.27 87.1
RE-1-1A-BH Back < e 100 < 100 100 0.0% 0.03 2.2
RE-1-JB-FH 1st Back < e 100 < 100 100 0.0% 0.03 2.2
Unspiked Sample;
Gas Vol. 14.7 dsl
RE-2-1A-FH Front e 259497 246858 253178 2.5% 2.19 148.6
RE-2-1A-BH Back < e 100 < 100 100 0.0% 0.03 2.2
RE-2-1B-FH 1st Back < e 100 < 100 100 0.6% 0.03 2.2
-------
LASCO Tube Samples Standard Curve from 5/1 9/97
Job NO. 97-3020 File: TUBEW2_3.WQ2
Initial Calibration:
Low Standard Mid Standard High Standard
Purity 99.0% Inj. Vol. 1.2 uL 6.0 uL 12.0 uL
Density 0.91 Std/Frt 1.1 3.9% 5.4 -1.6% 10.8 0.4%
Slope 288535.9 Peak Areas 313821 331638 1559010 1508366 3153635 3104427
Intcp -1359.5 Avg./Dev. 322729.5 2.8% 1533688 1.7% 3129031 0.8%
AvgRF 3.44E-06 RF 3.35E-06 3.5E-06 3.45E-06
Blank Avg 0 Note: Average area counts are reagent blank corrected
-------
f
•4
11
10-
9-
8
7
6
4
3
2-
1
0
STYRENE Calibration
322729.S
1533688
Area Counts
3129031
Styrene Calibration
Curve linearity check
Zero
Std1 tow
Std2 mid
Std3 high
uL
0
1.2
6
12
Regression Output:
Constant
StdErrofYEst
R Squared
No. of Observations
Degrees of Freedom
X Coefficient(s) 288700.8
Std Err of Coef. 4288.761
Corrected
0
1.08108
5.4054
10.8108
-2763.61
29567.12
0.999779
3
1
Area count
0 ;
322729.5
1533688
3129031
Corr. Coefficient
0.9998897
-------
Continuing Calibrations:
Concal
5/21/97
©10:34
Concal
5/21/97
@ 18:21
Concal
5/22/97
@2:26
Concal
5/22/97
Styrene
Styrene
Styrene
Styrene
Expected
Inject 1 Inject 2 Average Deviation Mass (mg) (mg)
1671766 1639020 1655393 1.0% 5.7
1749622 1820856 1785239 2.0% 6.2
1650673 1760397 1705535 3.2% 5.9
1781913 1813355 1797634 0.9% 6.2
5.9
5.9
5.9
5.9
Error
-3.4%
4.1%
-0.5%
4.9%
Concal
5/23/97
Concal
5/28/97
Concal 2
5/28/97
©17:29
Concal 2
5/30/97
@9:10
Concal 3
6/06/97
Styrene
Styrene
Styrene
Styrene
Styrene
1835350 1805627 1820489 0.8% 6.3
1628690 1579553 1604122 1.5% 5.6
1791912 1791912 1791912 0.0% 6.2
1874301 1819724 1847013 1.5% 6.4
1869258 1778858 1824058 2.5% 6.3
5.9
5.9
6.1
6.1
6.3
6.2%
-6.4%
1.5%
4.6%
0.3%
-------
Desorptlon Efficiency Study; Charcoal - 5/21/97 BHR
Styrene
Spike Level
(mg)
0
0.9009
4.5045
9.009
Inject 1 Inject 2
100 < 100
196351 199217
1053672 1027860
2104049 2203707
Desorp.
Average
100
197784
1040766
2153878
Deviation Mass (mg)
0.0%
0.7%
1.2%
—••** 2.3%
A'
0.01
0.69
3.61
7.47
i/erage
Efficiency
(blank corr.)
76.6%
80.2%
82.9%
79.9%
-------
Tube Results • STYRENE
Unspiked Sample
10-11-1
10-12-1
10-12^*
10-13-1
10-2-2
10-3-1
10-4-1
10-5-2
10-5-2
10-6-1
10-7-2
10-8-1
9-11-2
9-1 2-2*3 PT5
9-13-2
9-3-2
9-4-2
9-5-1
9-6-2
9-7-1
AF-12-1
AF-13-1
AF-5-2
AF-5-2
ME-11-1
ME-12-1
ME-13-2
ME-3-1
ME-3-2
ME-4-2
ME-5-1
ME-6-2
ME-7-1
ME-7-3
ME-8-1
ME-9-1
NDA-10-1
NDA-11-1
NDA-12-1
NDA-13-1
NDA-3-2
NDA-4-1
NDA-5-1
NDA-6-1
NDA-6-3
NDA-7-1
NDA-8-1
NDA-9-1
£ •
NDB-12^4 p0
NDB-3-3
Tube Section Inject 1
^ ,,„,„„,, ,.:.,,,,,„,,..,.,,
FH
FH
FH
FH
FH
FH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
1316659
367320
1223044
1552161
1858
< 100 <
< 100 <
426375
< 100 <
372292
641363
112707
< 100 <
16003
23684
13945
224232
25066
25154
< 100 <
248058
317929
< 100 <
292067
275585
197234
522127
688527
477292
428194
197782
425582
380856
489359
625243
561780
653
1031
< 100 <
24368
25328
25328
697
3369
< 100 <
< 100 <
2039
503
21106
4455
Inject 2
1201618
367320
1156430
1532526
1961
100 <
100 <
431523
100 <
365549
628193
117551
100 <
15616
27958
13869
217027
25525
24221
100 <
215052
253564
100 <
305172
291489
184270
501291
681005
448801
421774
200156
456713
389348
467190
623337
538755
558
1399
100 <
23442
25205
25205
652
3188
100 <
100 <
2163
501
18785
4077
Average
1259139
367320
1189737
1542344
1910
100
100
428949
100
368921
634778
115129
100
15810
25821
13907
220630
25296
24688
100
231555
285747
100
298620
283537
190752
511709
684766
463047
424984
198969
441148
385102
478275
624290
550268
606
1215
100
23905
25267
25267
675
3279
100
100
2101
502
19946
4266
Deviation Mass (mg)
4.6%
0.0%
2.8%
0.6%
2.7%
0.0%
0.0%
0.6%
0.0%
0.9%
1.0%
2,1%
0.0%
1.2%
8.3%
0.3%
1.6%
0.9%
1.9%
0.0%
7.1%
11.3%
0.0%
2.2%
2.8%
3.4%
2.0%
0.5%
3.1%
0.8%
0.6%
3.5%
1.1%
Z3%
0.2%
Z1%
7.8%
0.0%
0.0%
1.9%
0.2%
0.2%
3.3%
2.8%
0.0%
0.0%
3.0%
0.2%
5.8%
4.4%
4.37
1.28
4.13
5.35
0.01 DL
0.01 DL
0.01 DL
1.49
0.01 DL
1.28
2.20
0.40
0.01 DL
0.06
0.09
0.05
0.77
0,09
0.09
0.01 DL
0.81
1.00
0.01 DL
1.04
0.99
0.67
1.78
2.38
1.61
1.48
0.69
1.53
1.34
1.66
2.17
1.91
0.01 DL
0.01 DL
0.01 DL
0.09
0.09
0.09
0.01 DL
0,02
0.01 DL
0,01 DL
0.01 DL
0.01 DL
0.07
0.02
-------
NDB-4-2
NDB-5-2
NDB-7-2
NDB-8-2
RE-10-1
RE-11-1
RE-13-1
RE-3-1
RE-5-1
RE-5-1
RE-6-1
RE-7-1
RE-8-1
RE-9-1
FH
FH
FH
FH
FH
FH
FH
FH
BH
FH
FH
FH
FH
FH
< 100 <
< 100 <
2482
3347
28910
85960
207215
373486
< 100 <
232442
290765
69916
210373
102095
100 <
100 <
2490
3550
28751
90963
193557
337788
100 <
227643
271797
68914
211971
100765
100
100
2486
3449
28831
88462
200386
355637
100
230043
281281
69415
211172
101430
0.0%
0.0%
0.2%
2.9%
0.3%
2.8%
3.4%
5.0%
0.0%
1.0%
3.4%
0.7%
0.4%
0.7%
0.01
0.01
0.01
0.02
0.10
0.31
0.70
1.24
0.01
0.80
0.98
0.25
0.74
0.36
«
DL
DL
DL -> At or below the estimated limit of detection
-------
STYRENE Cylinder GC Results
Sample: Tube Section Inject 1
102S6L (102ppm) FH.BH
143.1S6L(143.1ppm) FH.BH
250.7S6L (250.7ppm) FH.BH
Six (6) liters drawn through all tubes
Inject 2
Average Deviation Mass (mg) ppm Found % of Cyl. Value
461442
537505
757613
553321
522005
749641
507382
529755
753627
9.1%
1.5%
0.5%
1.76
1.84
2.62
84.9
88.6
126.0
81.6%
61.9%
50.3%
/V7 .
/¥-/£/
wretif
/
,A
-------
Spiked Tube Results
Sample:
Tube Section
Inject 1
inject 2
Spiked Sample;
Gas Vol. 2.02 dsl
MES-3-3A Front
MES-3-3A Back <
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Theoretical Spike Cone. mg/CuM
Actual Spike Cone. (mg/CuM)
Unspiked Sample;
Gas Vol. 1.21 dsl
ME-3-3A Front
ME-3-3A Back <
Sample: Tube Section
lii:.,:} Ifx -V:: :?:•::;-:';; .•; • * ^;:"' '-?;:':':':;:';'
Spiked Sample;
Gas Vol. 1.95 dsl
RES-4-1A Front
RES-4-1A Back <
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Theoretical Spike Cone. mg/CuM
Actual Spike Cone. (mg/CuM)
UNSpiked Sample;
Gas Vol. 1.80 dsl
RE-4-1A Front
RE-4-1A Back <
742801
100
2.5
2.25
1114.98
1043.34
158837
100 <
Inject 1
121917
100 <
0.25
0.23
115.50
224.73
19431
100 <
782920
100
Average
762861
100
Deviation Mass (mg)
Spike Recovery %
Spike as % of Native Amount
162860
100
Inject 2
125805
100
160849
100
Average
123861
100
2.6%
0.0%
93.6%
198.4%
1.3%
0.0%
3.24
0.00
(mg/CuM)
1605.3
-2.1
0.68
0.00
Deviation Mass (mg)
Spike Recovery %
Spike as % of Native Amount
19358
100 <
19395
100
1.6%
0.0%
194.6%
267.2%
0.2%
0.0%
0.52
0.00
562.0
-3.6
(mg/CuM)
268.0
-2.2
0.08
0.00
43.2
-2.4
Pag«
-------
Spiked Tube Results
Sample:
Tube Section
Inject 1
Inject 2
Average
Deviation Mass (mg)
(mg/CuM)
Spiked Sample;
Gas Vol.
MES-6-2A
MES-6-2A
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Theoretical Spike Cone. mg/C
Actual Spike Cone. (mg/CuM)
Unspiked Sample;
Gas Vol.
ME-6-2A
ME-6-2A
Sample:
1.39 dsl
Spiked Sample;
Gas Vol.
AFS-5-2A
AFS-5-2A
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Theoretical Spike Cone. mg/C
Actual Spike Cone. (mg/CuM)
UNSpiked Sample;
Gas Vol.
AF-5-2A
AF-5-2A
Front
Back <
s(mg)
mg/CuM
CuM)
1.67 dsl
Front
Back <
Tube Section
7.01 dsl
Front
Back <
i(mg)
mg/CuM
CuM)
6.95 dsl
Front
Back <
778043
100 <
1.3
1.17
842.57
866.74
425582
100 <
Inject 1
535707
100 <
1.3
1.17
167.07
116.17
292067
100 <
651103
100
Spike Recovery
714573
100
%
Spike as % of Native Amount
456713
100
Inject 2
536639
100
Spike Recovery
441148
100
Average
536173
100
%
Spike as % of Native Amount
305172
100 <
298620
100
8.9%
0.0%
102.9%
91.7%
3.5%
0.0%
Deviation
0.1%
0,0%
69.5%
111.7%
2.2%
0.0%
2.48
0.01
1.53
0.01
Mass (mg)
1.86
0.01
1.04
0.01
1785.1
3.6
918.3
3.0
(mg/CuM)
265.8
0.7
149.6
0.7
Page 2
-------
Spiked Tube Results
Sample:
Tube Section
Inject 1
Inject 2
Average
Deviation Mass (mg)
Spiked Sample;
Gas Vol.
MES-11-2A
MES-11-2A
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Theoretical Spike Cone. mg/C
Actual Spike Cone. (mg/CuM)
UNspiked Sample;
Gas Vol.
ME-11-2A
ME-11-2A
2.52 dsl
(mg/CuM)
Front
Back <
i(mg)
mg/CuM
CuM)
2.41 dsl
Front
Back <
557483
100 <
0.95
0.86
339.63
287.38
336572
100 <
580495
100 <
568989
100
Spike Recovery %
Spike as % of Native Amount
351941
100 <
344257
100
2.0%
0.0%
84.6%
68.3%
2.2%
0.0%
1.98
0.01
1.20
0.01
784.4
2.0
497.0
2.1
Sample: Tube Section Ir
Spiked Sample;
Gas Vol. 3.01 dsl
RES-11-3A Front
RES-11-3A Back <
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Theoretical Spike Cone. mg/CuM
Actual Spike Cone. (mg/CuM)
UNspiked Sample;
Gas Vol. 3.57 dsl
RE-11-3A Front
RE-11-3A Back <
iject 1
106764
100 <
0.4
0.36
119.72
94.57
35176 .
100 <
Inject 2 Ave
115758
100
Spike Recovery %
Spike as % of Native
34420
100
rage
111261
100
Amount
34798
100
Deviation Mass (mg) '
4.0% 0.39
0.0% 0.01
79.0%
341.1%
1.1% 0.13
0.0% 0.01
(mg/CuM)
129.7
1.7
35.1
1.4
Pag
-------
Spiked Tube Results
Sample: Tube Section
Spiked Sample;
Gas Vol.
AFS-12-4A
AFS-12-4A
Spiked Vol (ul)
Theoretical Spiked Mass (mg)
Theoretical Spike Cone. mg/C
Actual Spike Cone. (mg/CuM)
UNspiked Sample;
Gas Vol,
AF-12-4A
AF-12-4A
Sample:
Spiked Sample;
Gas Vol.
MES-12-3A
MES-12-3A
Spiked Vol (ul)
Theoretical Spiked Mass {mg)
Theoretical Spike Cone. mg/C
Actual Spike Cone. (mg/CuM)
UNspiked Sample;
Gas Vol.
ME-12-3A
ME-12-3A
Inject 1
Inject 2
Average
Deviation Mass (mg)
(mg/CuM)
8.39 dsl
Front
Back <
Mmg)
mg/CuM
CuM)
9.22 dsl
Front
Back <
Tube Section
8.66 dsl
Front
Back <
•(mg)
mg/CuM
CuM)
8.28 dsl
Front
Back <
516297
100 <
0.67
0.60
71.94
49.15
461321
100 <
Inject 1
1269876
100 <
1.8
1.62
187.25
208.29
827233 .
100 <
560983
100
Spike Recovery
538640
100
%
Spike as % of Native Amount
461286
100
Inject 2
1555674
100
Spike Recovery
461304
100
Average
1412775
too
%
Spike as % of Native Amount
878962
100
853098
100
4.1%
0.0%
68.3%
41.4%
0.0%
0.0%
Deviation
10.1%
0.0%
111.2%
52.4%
3,0%
0.0%
187
0.01
1.60
0.01
. Mass (mg)
4.90
0.01
2.96
0.01
223.1
0.6
173.9
0.5
(mg/CuM)
565.9
0.6
357.7
0.6
Page 4
-------
(J. ZJL )
(I.52L)
\iot.
HI*
2+.059 IbGLC
- 25 J. 9 - 0259
on~rm
xO.5 =.
—
EXHW5T
-------
= 0.
(/20fl$ffi#W£)
- «~
0.91*0.99
-------
3 SO/) 5
A5
9.0 L
IOOO
- 3.2*75 *f OH
50% 5 'PIKE = I.
/.
0.91*03?
IMS-12-3
-------
/II/X/LI-AA7
30. K ><233m_ = fftffr o.
1000
C. 7J. OF to-.} fiyeevE t>iurnon
Art-) 2- f % 72
~ll - f 9.71
-------
LOU/
2.
1000
+.317*
-------
LASCO
Job No. 97-3020
Calibration:
Tube Samples
File: TUBE WK2.WQ2
Standard Curve from 5/19/97
Cumene
Purity
Density
Slope
intcp
AvgRF
Low Standard
99.9%
0.86
311862.7
-34792.2
3.29E-06
Inj. Vol.
Std./FJt
Peak Areas
Avg./Dev.
RF
1.5
1.3
425122
428664.5
3.01 E-06
uL
15.3%
432207
0.8%
Mid Standard
6.0
5.2
1413539
1395503
3.69E-06
uL
-11,0%
1377466
1.3%
High Standard
12.0
10.3
3301365
3261372
3.16E-06
uL
2.5%
3221358
1.2%
Blank Avg
0 Note: Average area counts are reagent blank corrected
-------
&
ID-
S'
8
7-
6
5
4
3
2
1
CUMENE Calibration
428664.5
1395502.5
Area Counti
3261371.5
Cumene Calibration
Curve linearity check
Zero
Std1 low
Std2 mid
Std3 high
uL
0
1.5
6
12
Regression Output:
Constant
StdErrofYEst
R Squared
No. of Observations
Degrees of Freedom
X Coefficient(s) 31 6605.5
Std Err of Coef. 31425.62
Corrected
0
1.28871
5.15484
10.30968
-72875.5
201138.1
0.990244
3
1
Area count
0
428664.5
1395503
3261372
Corr. Coefficient
0.9951 1
-------
Continuing Calibrations:
Expected
Concal
5/21/97 Cumene
@ 10:34
Concal
5/21/97 Cumene
©18:21
Concal
5/22/97 Cumene
@2:26
Concal
5/22/97 Cumene
Concal
5/23/97 Cumene
Concal
5/28/97 Cumene
@ 16:30
Concal 2
5/28/97 Cumene
Concal 2
5/30/97 Cumene
Concal 3
6/06/97 Cumene
©16:00
Inject 1 Inject 2 Average Deviation Mass(mg) (mg) Error
1531862 1500336 1516099 1.0% 5.0 5.2 -4.4%
1607211 1675417 1641314 2.1% 5.4 5.2 3.4%
1514010 1615963 1564987 3.3% 5.1 5.2 -1.4%
1641625 1667710 1654668 0.8% S.4 5.2 4.2%
1688369 1662881 1675625 0.8% 5.5 5.2 5.5%
1489575 1454962 1472269 1.2% 4.8 5.2 -7.1%
1649534 1649534 1649534 0.0% 5.4 5.2 3.9%
1730764 1678605 1704685 1.5% 5.6 5.2 7.3%
. 1662389 1749100 1705745 2.5% 5.6 5.2 7.3%
-------
Desorpt/on Efficiency Study; Cumene on Charcoal - 5/21/97 BHR
- Desorp.
Spike Level Efficiency
(mg) Inject 1 Inject 2 Average Deviation Mass (mg) (blank corr.)
0 < 100 <
0.86 247201
4.3 1200100
8.6 2313958
100
250869
1173132
2420783
2859174
10
249035
1186616
2367371
900.0%
0.7%
1.1%
2.3%
0.11
0.91
3.92
7.70
Average
105.8%
91.1%
89.6%
95.5%
-------
Tube Results - CUMENE
Unspiked Sample
10-11-1
10-12-1
10-12-4
10-13-1
10-2-2
10-3-1
10-4-1
10-5-2
10-5-2
10-6-1
10-7-2
10-8-1
9-11-2
9-12-/3 fY4
9-13-2
9-3-2
9-4-2
9-5-1
9-6-2
9-7-1
AF-12-1
AF-13-1
AF-5-2
AF-5-2
ME-11-1
ME-12-1
ME-13-2
ME-3-1
ME-3-2
ME-4-2
ME-5-1
ME-6-2
ME-7-1
ME-7-3
ME-8-1
ME-9-1
NDA-10-1
NDA-11-1
NDA-12-1
NDA-13-1
NDA-3-2
NDA-4-1
NDA-5-1
NDA-6-1
NDA-6-3
NDA-7-1
NDA-8-1
NDA-9-1
NDB-12-J/4 (**
NDB-3-3 ny
Tube Section
FH
BH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
Inject 1 Inject 2 Average Deviation Mass(mg)
1087
100 <
3765
100 <
1412
100 <
100 <
100 <
100 <
100 <
552
100 <
100 <
100 <
100 <
100 <
100 <
100 <
100 <
1066
100 <
100 <
100 <
100 <
100 <
100 <
100 <
1050
100 <
1377
100 <
100 <
831
1167
1894
100 <
1485
499
100 <
1302
1379
8229
100 <
100 <
100 <
100 <
8147
100 <
704
100 <
375
100 <
2456
100 <
468
100 <
100 <
100 <
100 <
100 <
471
100 <
100 <
100 <
100 <
100 <
100 <
100 <
100 <
1051
100 <
100 <
100 <
100 <
100 <
100 <
100 <
778
100 <
2080
100 <
100 <
1278
1221
1643
100 <
1928
510
100 <
444
1757
8650
100 <
100 <
100 <
100 <
8147
100 <
632
100 <
731
100
3111
100
940
100
100
100
100
100
512
100
100
100
100
100
100
100
100
1059
100
100
100
100
100
100
100
914
100
1729
100
100
1055
1194
1769
100
1707
505
100
873
1568
8440
100
100
100
100
8147
100
668
100
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.7%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
Z5%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
5.4%
0.0%
0.11 DL
0.11 DL
0.12 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.12 DL
0.11 DL
0.11 DL
0.11 DL
0.12 DL
0.12 DL
0.11 DL
0.12 DL
0.11 DL
0.11 DL
0.11 DL
0.12 DL
0.14
0.11 DL
0.11 DL
0.11 DL
0.11 DL
0.14
0.11 DL
0.11 DL
0.11 DL
-------
NDB-4-2 FH
NDB-5-2 FH
NDB-7-2 FH
NDB-8-2 FH
RE-10-1 FH
RE-11-1 FH
RE-13-1 FH
RE-3-1 FH
RE-5-1 FH
RE-5-1 FH
RE-6-1 FH
RE-7-1 FH
RE-8-1 FH
RE-9-1 FH
DL -> At or below the estimated limit of detection
100 <
100 <
3079
100 <
4812
100 <
611
100 <
100 <
1402
100 <
100 <
100 <
100 <
100 <
100 <
2574
100 <
4706
100 <
545
100 <
•100 <
1319
100 <
100 <
100 <
100 <
100
100
2827
100
4759
100
578
100
100
1361
100
100
100
100
0.0%
0.0%
0.0%
0.0%
1.1%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.11
0.11
0.12
0.11
0.13
0.11
0.11
0.11
0.11
0.12
0.11
0.11
0.11
0.11
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
-------
LASCOi
Job No. 97-3020
Calibration:
Tube Samples
File: TUBE WK2.WQ2
Standard Curve from 5/19/97
Methyl Methacrylate
Purity
Density
Slope
Intcp
AvgRF
99.0%
0.936
166775.9
-5619.1
5.81 E-06
Inj. Vol.
Std/Frt
Peak Areas
Avg,/Dev.
RF
Low Standard
1.2
1.1
235866
237059.5
4.69E-06
lit
30.9%
238253
0.5%
Mid Standard
6,0
5.6
832159
807377.5
6.89E-06
uL
-12.3%
782596
3.1%
High Standard
12.0
11.1
1925615
1900278
5.85E-06
uL
2.8%
1874940
1.3%
Blank Avg
0 Note: Average area counts are reagent blank corrected
-------
MMA Calibration
12
_i 10-
237059.5
807377.5
Area Counts
1900277.5
Methyl Methacrylate Calibration
Curve linearity check uL
Zero 0
Std1 low 1 .2
Std2 mid 6
Std3high 12
Regression Output:
Constant
Std Err of Y Est
R Squared
No. of Observations
Degrees of Freedom
X Coefficients) 1 66544.2
Std Err of Coef. 16488.78
Corrected
0
1.111968
5.55984
11.11968
-2078.49
117422.7
0.990293
3
1
Area count
0
237059.5
807377.5
1900278
Corn Coefficient
0.995135
-------
Continuing Calibrations:
Expected
Concal
5/21/97
@ 10:34
Concal
5/21/97
@ 23:30
Concal
5/22/97
Concal
5/22/97
Concal
5/22/97
Concal
5/28/97
Concal 2
5/28/97
@17:29
Concal 2
5/30/97
Concal 3
6/06/97
Inject 1 Inject 2 Average Deviation Mass (mg) (mg)
Methyl Methacrylat 735470 732471 733971 0.2% 4.4 4.6
Methyl Methacrylat 757277 787351 772314 1.9% 4.7 4.6
Methyl Methacrylat 713704 754327 734016 2.8% 4.4 4.6
Methyl Methacrylat 746430 762476 754453 1.1% 4.6 4.6
Methyl Methacrylat 760730 735306 748018 1.7% 4.5 4.6
Methyl Methacrylat 758935 737574 748255 1.4% 4.5 4.6
Methyl Methacrylat 919220 919220 919220 0.0% 5.5 5.6
Methyl Methacrylat 916432 916432 916432 0.0% 5.5 5.6
Methyl Methacrylat 703764 669425 686595 2.5% 4.2 4.4
Error
-4.3%
0.7%
-4.3%
-1.6%
-2.5%
-2.4%
-0.3%
-0.6%
-6.7%
-------
Desorpf/on Efficiency Study; MM A on Charcoal • 5/21/97 BHR
Oesorp.
Spike Level Efficiency
(mg) Inject 1 Inject 2 Average Deviation Mass (mg) (blank corr.)
0 < 100 < 100 100 0.0% 0.03
0.92664 93793 95070 94432 0.7% 0.60 64.7%
4.6332 552721 538699 545710 1.3% 3.31 71.4%
9.2664 1117140 1175094 1146117 2.5% 6.91 74.5%
: Average 70.2%
-------
Tube Results • METHYL METHACRYLATE
Unspiked Sample
10-11-1
10-12-1
10-12-4
10-13-1
10-2-2
10-3-1
10-4-1
10-5-2
10-5-2
10-6-1
10-7-2
10-8-1
9-11-2
9-12/J PTS
9-13-2
9-3-2
9-4-2
9-5-1
9-6-2
9-7-1
AF-12-1
AF-13-1
AF-5-2
AF-5-2
ME-11-1
ME-12-1
ME-13-2
ME-3-1
ME-3-2
ME-4-2
ME-5-1
ME-6-2
ME-7-1
ME-7-3
ME-8-1
ME-9-1
NDA-10-1
NDA-11-1
NDA-12-1
NDA-13-1
NDA-3-2
NDA-4-1
NDA-5-1
NDA-6-1
NDA-6-3
NDA-7-1
NDA-8-1
NDA-9-1
NDB-12-^4 -^t
NDB-3-3 n
Tube Section
FH
BH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
Inject 1
43376
100 <
11724
100 <
31430
100 <
405
100 <
1882
1983
21970
100 <
100 <
1860
31733
535
7050
100 <
100 <
408
100 <
100 <
100 <
100 <
100 <
100 <
432
5865
100 <
1275
100 <
11634
42390
56351
13137
100 <
100 <
300
100 <
972
358
100 <
451
100 <
339
100 <
100 <
441
100 <
100 <
Inject 2
44832
100 <
11888 <
100 <
30702
100 <
537
100 <
1920
2369
22108
100 <
100 <
1798
40474
515
6951
100 <
100 <
411
100 <
100 <
100 <
100 <
100 <
100 <
421
5304
100 <
1254
100 <
11406
43533
53320
12825
100 <
100 <
296
100 <
779
302
100 <
487
100 <
362
100 <
100 <
387
100 <
100 <
Average Deviation Mass (mg)
44104
100
11806
100
31066
100
471
100
1901
2176
22039
100
100
1829
36104
525
7001
100
100
410
100
100
100
100
100
100
427
5585
100
1265
100
11520
42962
54836
12981
100
100
298
100
876
330
100
469
100
3S1
100
100
414
100
100
1.7%
0.0%
0.7%
0.0%
1.2%
0.0%
0.0%
0.0%
1.0%
8.9%
0.3%
0.0%
0.0%
1.7%
12.1%
0.0%
0.7%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
1.3%
5.0%
0.0%
0.0%
0.0%
1.0%
1.3%
2.8%
1.2%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.30
0.03
0.10
0.03
i 0.22
0.03
0.04
0.03
0.05
0.05
0.17
0.03
0.03
0.04
0.25
0.04
0.08
0.03
0.03
0.04
0.03
0.03
0.03
0.03
0.03
0.03
0.04
0.07
0.03
0.04
0.03
0.10
0.29
0.36
0.11
0.03
0.03
0.04
0.03
0.04
0.04
0.03
0.04
0.03
0.04
0.03
0.03
0.04
0.03
0.03
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
-------
NDB-4-2 FH <
NDB-5-2 FH <
NDB-7-2 FH <
NDB-8-2 FH <
RE-10-1 FH <
RE-11-1 FH <
RE-13-1 FH
RE-3-1 FH
RE-5-1 FH
RE-5-1 FH
RE-6-1 FH <
RE-7-1 FH <
RE-8-1 FH <
RE-9-1 FH 1730 1656 1693 2.2% 0.04
DL ~> At or below the estimated limit of detection
100 <
100 <
100 <
100 <
100 <
100 <
602
1092
227§
1135
100 <
100 <
100 <
100 <
100 <
100 <
100 <
100 <
100 <
557
1036
1988
1090
100 <
100 <
100 <
100
100
100
100
100
100
580
1064
2134
1113
100
100
100
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
6.8%
0.0%
0.0%
0.0%
0.0%
0.03
0.03
0.03
0.03
0.03
0.03
0.04
0.04
0.05
0,04
; 0.03
0.03
0.03
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
DL
-------
LASCO Bag Samples
Standard Curve From 5/14/97
Curve
Analyte (ppmv)
Methane
Density 1
Purity 100.0%
Slope 380.2
Intcp -543. 6
Response Factors
Avg. Response factor
ppmv
Std./Fit
Peak Areas
Avg./Dev.
2.74E-03
Stdl
Sid 2
Std3
1
100.0%
380.2
-543.6
ppmv
Std./Fit
Peak Areas
Avg./Dev.
2.74E-03
24.9
8604
8634
2.89E-03
-3.1%
8664
0.3%
87.2
32195
32295.5
2.70E-03
49.8
19338
-1.0%
32396
0.3%
18620
510.4
195060
193591
2.64E-03
87.2
32195
0.0%
192122
0.8%
32396
Ethane
Stdl
Sid 2
Sid 3
Density
Purity
Slope
Intcp
Response Factors
Avg. Response factor
0.79
99.8%
632.0
-68.9
ppmv
Std./Fit
Peak Areas
Avg./Dev.
5.0
2942
2954
1.69E-03
-4.3%
2966
0.4%
9.0
5668
5686.5
1.58E-03
1.2%
5705
0.3%
99.0
63629
62499.5
1.58E-03
0.0%
61370
1.8%
1.62E-03
-------
ASCO Bag Samples
Standard Curve From 5/14/97
con-cal
5/14/97
@20:07
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (pptnv)
Expected (ppmv)
Error %
Methane
17271
18551
3.6%
48.5
49.83
-2.7%
Ethane
57019
61099
3.5%
93.6
99
-5.8%
con-cal
5/15/97
@ 12:08
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (Mg/CuM)
Expected (Mg/CuM)
Error %
Methane
18669
19131
1.2%
51.1
49.83
2.6%
Ethane
61320
62793
1.2%
98.3
99
-0.7%
Run 1 Open 9
Bag
Cl
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
108487
105427
1.4%
282.7
188.1
Ethane
4482
4375
1.2%
7.1
8.9
Run 1 Open 10
Bag
Cl
Run 2 Open 9
Bag
Cl
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Methane
32471
29629
4.6%
83.1
55.3
Methane
117443
119755
1.0%
3133
Ethane
1886
1731
4.3%
3.1 RF
3.8
Ethane
4766
4858
1.0%
7.7
-------
ASCO Bag Samples
Standard Curve From 5/14/97
Measured (Mg/CuM)
208.4
9.6
Run 2 Open 10
Bag
Unspiked
Cl
R2 Open 10
Bag Spike
Cl
Open 10
Run 3
Cl
Open 9
Run 3
Cl
Open 10
Runl
C2 _
Inject 1 (AC)
Inject 2 (AC)
Inject 3 (AC)
Inject 4 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Initial Volume (1)
Final Volume (1)
Spike Cone (ppmv)
Spike Voi (1)
Expected Cone, (ppmv)
Spike Recovery %
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
34381
33904
34934
33165
2.7%
91.2
60.7
Methane
27032
27177
0.3%
72.7
2
4
49.83
2.0000
70.53
103.1%
Methane
32240
32807
0.9%
87.0
57.8
Methane
112227
120588
3.6%
307.6
204.6
Methane
29265
31523
3.7%
81.4
54.1
Ethane
1937
1914
1970
1872
2.7%
3.3 RF
4.1
Ethane
43565
43800
0.3%
69.2
2
4
l.OE+06
0.0100
75.88
91.2%
Ethane
1850
1848
0.1%
3.1 RF
3.9
Ethane
4613
4923
3.3%
7.7
9.5
Ethane
1717
1849
3.7%
3.0
3.8
-------
ASCO Bag Samples
Standard Curve From 5/14/97
Open 9
Runl
C2
Open 9
Run 2
C2
Open 10
Run 2
C2
Open 10
Run 3
C2
Open 9
Run 3
C2
Open 9
Runl
C3
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AQ
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
86375
88076
1.0%
230.8
153.5
Methane
82117
80850
0.8%
215.7
143.5
Methane
28642
28793
0.3%
77.0
51.2
Methane
31605
31923
0.5%
85.0
56.5
Methane
99055
99985
0.5%
263.2
175.0
Methane
58330
58408
0.1%
154.9
103.1
Ethane
3634
3707
1.0%
5.9
7.4
Ethane
3595
3532
0.9%
5.7
7.2
Ethane
6158
6187
0.2%
9.9
12.3
Ethane
1879
1893
0.4%
3.2
4.0
Ethane
4290
4332
0.5%
6.9
8.6
Ethane
2481
2476
0.1%
4.2
5.2
-------
ASCO Bag Samples
Standard Curve From 5/14/97
Open 10
Runl
C3
Run 2
C3
Open 10
Run 3
C3
Open 9
Run 3
C3
Open 10
Runl
C4
Open 9
Runl
C4
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
18751
18235
1.4%
50.1
33.3
Methane
104518
104518
0.0%
276.3
183.8
Methane
17640
18343
2.0%
48.7
314
Methane
93350
88748
2.5%
240.9
160.2
Methane
20001
20989
2.4%
553
36.8
Methane
97436
98149
0.4%
258.6
172.0
Ethane
1573
1518
1.8%
2.6
3.3
Ethane
4190
4190
0.0%
6.7
8.4
Ethane
1435
1496
2.1%
2.5
3.1
Ethane
3727
3548
2.5%
5.9
7.3
Ethane
1582
1664
2.5%
2.7
3.4
Ethane
4125
4128
0.0%
6.6
83
-or
Open 10
Methane
Ethane
-------
ASCO Bag Samples
Standard Curve From 5/14/97
Run 2
C4
Open 9
Run 2
C4
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
22526
21186
3.1%
58.9
39.2
Methane
97652
94425
1.7%
254.0
169.0
1797
1691
3.0%
3.0
3.7
Ethane
4236
4115
1.4%
6.7
8.4
-------
LASCO Bag Samples
Standard Curve From 5/19/97
Curve
Analyte (ppmv)
Methane
Stdl
Std2
Std3
Density
Purity
Slope
Intcp
Response Factors
Avg. Response factor
Ethane
1
100.0%
364.7
2534.9
ppmv
StdTFit
Peak Areas
Avg./Dev.
2.48E-03
29.9
13777
13381.5
2.23E-03
-0.5%
12986
3.0%
174.4
71464
70077
2.49E-03
49.8
19338
6.2%
68690
2.0%
18620
510.4
189780
187348.5
2.72E-03
87.2
32195
-0.7%
184917
1.3%
32396
Stdl
Ski 2
Std3
Density
Purity
Slope
Intcp
Response Factors
Avg. Response factor
0.79
99.8%
542.4
202.5
ppmv
Std./Fit
Peak Areas
Avg./Dev.
4.0
2302
2295.5
1.74E-03
-3.5%
2289
0.3%
10.7
6426
6313.5
1.69E-03
5.3%
6201
1.8%
107.0
58972
58213.5
1.84E-03
-0.0%
57455
1.3%
1.76E-03
-------
con-cal
5/19/97
@19:15
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Expected (ppmv)
Error %
Methane
64816
64271
0.4%
170.0
174.4
-2.6%
Ethane
5884 Second Bag (midrange)
5810
0.6%
10.4
10.7
-2.8%
con-cal
5/20/97
@16:37
Methane
Ethane
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (Mg/CuM)
Expected (Mg/CuM)
Error %
63187
64599
1.1%
1682
174.4
-3.7%
5745
5868
1.1%
10.3
10.7
-3.6%
Open 9
Runl
Cond.5
5/19/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
125902
126728
0.3%
339.4
225.7
Ethane
5117
5169
0.5%
9.1
11.4
Open 10
Runl
Cond.5
5/19/97
Open 9
Run 2
Cond.5
5/19/97
Open 10
Run 2
CondJ
5/19/97
Methane
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
22818
24500
3.6%
57.9
38J
Ethane
18342
16781
4.4%
41.2
27.4
Methane
117354
119232
0.8%
317.4
211.1
1049
962
4.3%
1.8 RF
2.2
Ethane
4805
4897
0.9%
8.6
10.7
Ethane
1261
1319
22%
22 RF
Open 9
Run 3
CowLS
5/19/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Methane
102146
102868
0.4%
Ethane
4098
4119
03%
-------
Open 10
Run 3
Cond.5
5/19/97
Open 9
Runl
Cond.6
5/19/97
Open 10
Runl
Cond.6
5/19/97
Open 9
Run 2
Cond.6
5/19/97
Open 10
Run 2
Cond.6
5/19/97
Open 9
Run 3
Cond.6
5/19/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
13822
13822
0.0%
30.9
20.6
Methane
84288
78405
3.6%
216.1
143.7
Methane
16205
16410
0.6%
37.8
25.1
Methane
106894
104139
1.3%
282.4
187.8
Methane
25129
23202
4.0%
59.3
39.4
Methane
102608
105189
1.2%
277.9
184.9
Ethane
745 L
745
0.0%
1.3 F
1.6
Ethane
3454
3230
3.4%
5.8
7.2
Ethane
895
903
0.4%
1.6
2.0
Ethane
4370
4261
1.3%
7.6
9.5
Ethane
1362
1251
4.2%
2J
2.8
Ethane
4163
4249
1.0%
7.4
9.2
745 Leak in Bag detected
-------
Open 10
Run3
Cond.6
5/19/97
Open 9
Runl
Cond.7
5/20/97
Open 10
Runl
Cond.7
5/20/97
Open 9
Run 2
Cond.7
5/20/97
Open 10
Run 2
Cond.7
5/20/97
Open 9
Run3
Cond.7
5/20/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AQ
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
21997
20500
3.5%
51.3
34.1
Methane
112319
114910
1.1%
304.6
202.6
Methane
21062
20324
1.8%
49.8
33.1
Methane
75045
76569
1.0%
200.9
133.6
Methane
17505
17726
0.6%
41.3
27.5
Methane
71308
68186
2.2%
184.3
122.6
Ethane
1149
1080
3.1%
1.9
2.4
Ethane
4567
4611
0.5%
8.1
10.1
Ethane
1120
1088
1.4%
1.9
2.4
Ethane
3088
3129
0.7%
5.4
6.7
Ethane
933
935
0.1%
1.6
2.0
Ethane
2897
2762
2.4%
4.8
6.0
-------
Open 10
Run 3
Cond.7
5/20/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
17249
16656
1.7%
39.5
263
Ethane
939
885
3.0%
1.6
10
-------
LASCO Bag Samples
Standard Curve From 5/22/97
Curve
Analyte (ppmv)
Methane
Std 1
Std2
Std 3
Density
Purity
Slope
Intcp
Response Factors
Avg. Response factor
1
100.0%
312.0
431.2
ppmv
Std./Fit
Peak Areas
Avg./Dev.
0.003175
49.8 -3.0%
15477 15535.00
15506 0.2%
0.00321
174.4
55987
56143
0.00311
49.8
19338
2.4%
56299
0.3%
18620
510.4
156054
159270.5
0.00320
87.2
32195
-0.3%
162487
2.0%
32396
Ethane
Std 1
Std 2
Std 3
Density
Purity
Slope
Intcp
Response Factors
Avg. Response factor
0.79
99.8%
508.7
-237.3
ppmv
Std./Fit
Peak Areas
Avg./Dev.
6.6
3301
3307
0.00199
5.9%
3313
0.2%
*
10.00
4479
4384.5
0.00228
-9.2%
4290
2.2%
*
107.0
53094
54228.5
0.00197
0.1%
55363
2.1%
0.0020812
Page
-------
LASCO Bag Samples
con-cal
5/22/97
11:23 Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Expected (ppmv)
Error %
Standard Curve From 5/22/97
Methane
16365
15900
1.4%
50.3
49.8
1.0%
Ethane
6070 Second Bag, 11 mL 1.07%E,
5751 10LBal.49.8M
2.7%
12.1
11.8
2.6%
con-cal
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Expected (ppmv)
Error %
Methane
15638
15638
0.0%
48.7
49.8
-2.2%
Ethane
5838
5838
0.0%
11.9
11.8
1.4%
con-cal
5/29/97
7:35
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Expected (ppmv)
Error %
Methane
14619
14922
1.0%
46.0
49.8
-8.4%
Ethane
5067 Second Bag, 10 mL 1.07%E,
5166 10LBal.49.8M
1.0%
.10.5
10.7
-1.7%
con-cal
5/29/97
20:15
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (Mg/CuM)
Expected (Mg/CuM)
Error %
Methane
15069
14515
1.9%
46.0
49.8
-8.2%
Ethane
5202
5027
1.7%
10.5
10.7
-1.7%
Oven 10
Run 1
Cond.8
5/22/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
18811
18879
0.2%
59.0
39.3
Ethane
1478
1477
0.0%
2.9
3.7
Page 2
-------
LASCO Bag Samples
Oven 9
Run 2
Cond.8
5/22/97
Standard Curve From 5/22/97
Oven 9
Run 1
Cond.8
5/22/97
Oven 10
Run 2
Con4.8
5/22197
Oven 9
Run 3
Cond.8
5/22/97
Oven 10
Run 3
Cond.8
5/22/97
Oven 9
Run 1
Cond.9
5/22/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
101712
102614
0.4%
326.1
216.9
Methane
103959.
103959
0.0%
331.8
220.7
Methane
19737
20239
1.3%
62.7
41.7
Methane
90911
91681
0.4%
291.2
193.7
Methane
16968
16968
0.0%
53.0
35.3
Methane
40419
37234
4.1%
123.1
81.9
Ethane
3971
4011
0.5%
8.3
10.4
Ethane
4216
4216
0.0%
8.8
10.9
Ethane
1406
1429
0.8%
2.8
3.5
Ethane
3601
3571
0.4%
7.5
9.4
Ethane
1346
1346
0.0%
2.7
3.3
Ethane
1790
1647
4.2%
3.4
4.3
Page 3
-------
LASCO Bag Samples
Oven 10
Standard Curve From 5/22/97
Run 1
Cond.9
5/22/97
Oven 9
Run 1
Cond.10
5/22/97
Oven 10
Run 1
Cond.10
5/22/97
Oven 9
Run 1
Cond.ll
5/23/97
Oven 10
Run 1
Cond.ll
5/23/97
Oven 9
Run 2
Cond.ll
5/23/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject I (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
11779
11044
3.2%
36.7 R
24.4
Ethane
777
723
3.6%
1.5
1.9
Methane
59090
60892
1 .5%
190.9
127.0
Methane
19083
18982
0.3%
59.6
39.7
Methane
52339
49733
2.6%
162.2
107.9
Methane
21969
20647
3.1%
66.9
44.5
Methane-
48032
47098
1.0%
151.1
100.5
Ethane
2430
2472
0.9%
4.9
6.1
Ethane
1282
1273
0.4%
2.5
3.2
Ethane
2329
2228
2.2%
4.5
5.7
Ethane
1485
1409
2.6%
2.9
3.6
Ethane
2102
2081
0.5%
4.2
5.2
Page 4
-------
LASCO Bag Samples
Oven 10
Run 2 Inject 1 (AC)
Cond.ll Inject 2 (AC)
5/23/97 Deviation
Measured (ppmv)
Measured (Mg/CuM)
Standard Curve From 5/22/97
Oven 9
Run 3
Cond.ll
5/23/97
Oven 10
Run 3
Cond. 11
5/23/97
Oven 10
Run, I
Cond. 12
5/29/97
Oven 9
Run 1
Cond. 12
5/29/97
Oven 9
Run 3
Cond. 12
5/29/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject I (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
13808
14298
1.7%
45.2 R
30.0
Ethane
930
960
1.6%
1.9
2.3
Methane
52973
52973
0.0%
168.4
112.0
Methane
19854
20001
0.4%
62.5
41.6
Methane
18366
16669
4.8%
54.8
36.4
Methane
66302
64000
1.8%
207.4
138.0
Methane
87352
88406
0.6%
280.3
186.4
Ethane
2278
2278
0.0%
4.5
5.7
Ethane
1246
1248
0.1%
2.5
3.1
Ethane
1476
1341
4.8%
2.8
3.5
Ethane
3138
3042
1.6%
6.1
7.7
Ethane
4035
4086
0.6%
8.4
10.5
PageS
-------
LASCO Bag Samples
Oven 10
Run 3 Inject 1 (AC)
Cond.12 Inject 2 (AC)
5/29/97 Deviation
Measured (ppmv)
Measured (Mg/CuM)
Standard Curve From 5/22/97
Oven 9
Run 4
Cond,12
5/29/97
Oven 10
Run 4
Cond.12
5/29/97
Oven 9
Run 1
Cond.13
5/29/97
Oven 10
Run 1
Cond.13
5/29/97
Oven 9
Run 2
Cond.13
5/29/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Methane
15369
14820
1.8%
48.5 R
32.3
Ethane
1264
1215
2.0%
2.5
3.1
Methane
80294
80787
0.3%
256.8
170.8
Methane
18933
18906
0.1%
59.3
39.4
Methane
87617
80318
4.3%
267.8
178.1
Methane
19900
19813
0.2%
62.3
41.4
Methane
91663
90948
0.4%
291.3
193.7
Ethane
3725
3758
0.4%
7.8
9.8
Ethane
1565
1550
0.5%
3.1
3.9
Ethane
4077
3758
4.1%
8.2
10.2
Ethane
1621
1557
2.0%
3.2
3.9
Ethane
4251
4203
0.6%
8.8
10.9
Page 6
-------
LASCO Bag Samples
Oven 10
Run 2 Inject 1 (AC)
Cond.13 Inject 2 (AC)
5/29/97 Deviation
Measured (ppmv)
Measured (Mg/CuM)
Oven 9
Run 3
Cond.13
5/29/97
Oven 10
Run 3
Cond.13
5/29/97
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Inject 1 (AC)
Inject 2 (AC)
Deviation
Measured (ppmv)
Measured (Mg/CuM)
Standard Curve From 5/22/97
Methane Ethane
18758 1532
18758 1532
0.0% 0.0%
58.7 3.0
39.1 3.8
Methane Ethane
73908 3360
73908 3360
0.0% 0.0%
235.5 7.1
156.6 8.8
Methane Ethane
12497 1005
13126 1076
2.5% 3.4%
41.2 R 2.1
27.4 2.6
Page?
-------
LASCO
Job No. 97-3020
Tube Results • STYRENE
Tube Samples
File: TUBE WK2.WQ2
Standard Curve from 5/19/97
Unspiked Sample Tube Section Inject 1 Inject 2 Average
10-2-2
10-3-1
10-4-1
10-5-2
10-5-2
10-6-1
10-7-2
9-3-2
9-4-2
9-5-1
9-6-2
9-7-1
AF-5-2
AF-5-2
ME-3-1
ME-3-2
ME-4-2
ME-5-1
ME-6-2
ME-7-1
ME-7-3
ME-8-1
NDA-3-2
NDA-4-1
NDA-5-1
NDA-6-1
NDA-6-3
NDA-7-1
NDA-8-1
NDB-3-3
NDB-4-2
NDB-5-2 '
NDB-7-2
RE-3-1
RE-5-1
RE-5-1
RE-6-1
RE-7-1
RE-8-1
FH
FH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
BH
FH
FH
FH
FH
1858
< 100 <
< 100 <
< 100 <
426375
372292
641363
13945
224232
25066
25154
< 100 <
292067
< 100 <
688527
477292
428194
197782
425582
380856
489359
625243
25328
25328
697
3369
< 100 <
< 100 <
2039
4455
< 100 <
< 100 <
2482
373486
< 100 <
232442
290765
69916
210373
1961
100 <
100 <
100 <
431523
365549
628193
13869
217027
25525
24221
100 <
305172
100 <
6810Q5
448801
421774
200156
456713
389348
467190
623337
25205
25205
652
3188
100 <
100 <
2163
4077
100 <
100 <
2490
337788
100 <
227643
271797
68914
211971
1910
100
100
100
428949
368921
634778
13907
220630
25296
24688
100
298620
100
684766
463047
424984
198969
441148
385102
478275
624290
25267
25267
675
3279
100
100
2101
4266
100
100
2486
355637
100
230043
281281
69415
211172
Deviation Mass (mg)
2.7%
0.0%
0.0%
0.0%
0.6%
0.9%
1.0%
0.3%
1.6%
0.9%
1.9%
0.0%
2.2%
0.0%
0.5%
3.1%
0.8%
0.6%
3.5%
1.1%
2.3%
0.2%
0.2%
0.2%
3.3%
2.8%
0.0%
0.0%
3.0%
4.4%
0.0%
0.0%
0.2%
5.0%
0.0%
1.0%
3.4%
0.7%
0.4%
0.01
0.01
0.01
0.01
1.49
1.28
2.20
0.05
0.77
0.09
0.09
0.01
1.04
0.01
2.38
1.61
1.48
0.69
1.53
1.34
1.66
2.17
0.09
0.09
0.01
0.02
0.01
0.01
0.01
0.02
0.01
0.01
o.ot
1.24
0.01
0.80
0.98
0.25
0.74
-------
LASCO
Job No. 97-3020
Tube Results • CUMENE
Tube Samples
File: TUBE WK2.WQ2
Standard Curv
Unspiked Sample
10-2-2
10-3-1
10-4-1
10-5-2
10-5-2
10-6-1
10-7-2
9-3-2
9-4-2
9-5-1
9-8-2
9-7-1
AF-5-2
AF-5-2
ME-3-1 .
ME-34 ' '
ME-4-2
ME-5-1
ME-6-2
ME-7-1
ME-7-3
ME-8-1
NDA-3-2
NDA-4-1
NDA-5-1
NDA-6-1
NDA-6-3
NDA-7-1
NDA-8-1
NDB-3-3
NDB-4-2
NDB-5-2
NDB-7-2
RE-3-1
RE-5-1
RE-5-1
RE-6-1
Ri-7-1
RE-8-1
Tube Section
FH
BH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
Inject 1
I
1087
100 <
3765
100 <
1412
100 <
100 <
100 <
100 <
100 <
552
100 <
100 <
100 <
100 <
100 <
100 <
100 <
100 <
1066
100 <
100 <
100 <
100 <
100 <
100 <
100 <
1050
100 <
1377
100 <
100 <
831
1167
1894 ,
100 <
1485
499
100 <
Inject 2
375
100 <
2456
100 <
468
100 <
100 <
100 <
100 <
100 <
471
100 <
100 <
100 <
100 <
100 <
100 <
100 <
100 <
1051
100 <
100 <
100 <
100 <
100 <
100 <
100 <
778
100 <
2080
100 <
100 <
1278
1221
1643
100 <
1928
510
100 <
Average Deviation Mass (mg)
731
100
3111
100
940
100
100
100
100
100
512
100
100
100
100
100
100
100
100
1059
100
100
100
100
100
100
100
914
100
1729
100
100
1055
1194
1769
100
1707
505
100
48.7%
0.0%
21.0%
0.0%
50.2%
0.0%
0.0%
0.0%
0.0%
0.0%
7.9%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.7%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
0.0%
14.9%
0.0%
20.3%
0.0%
0.0%
21.2%
2.3%
7.1%
0.0%
13.0%
1.1%
0.0%
0.11
0.11
6.12
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.11
0.12
0.11
0.11
0.11
0.12
0.12
0.11
0.12
0,11
0.11
-------
LASCO Tube Samples
JOb NO. 97-3020 File: TUBE_WK2.WQ2
Tube Results • METHYL METHACRYLATE
Standard Curv
Unspiked Sample
10-2-2
10-3-1
10-4-1
10-5-2
10-5-2
10-6-1
10-7-2
9-3-2
9-4-2
9-5-1
9-6-2
9-7-1
AF-5-2
AF-5-2
ME-3-1
ME-3-2
ME-4-2
ME-5-1
ME-6-2
ME-7-1
ME-7-3
ME-8-1
NDA-3-2
NDA-4-1
NDA-5-1
NDA-6-1
NDA-6-3
NDA-7-1
NDA-8-1
NDB-3-3
NDB-4-2
NDB-5-2
NDB-7-2
RE-3-1
RE-5-1
RE-5-1
RE-6-1
RE-7-1
RE-8-1
Tube Section
FH
'BH
FH
BH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
FH
Inject 1
43376
100 <
11724
100 <
31430
100 <
405
100 <
1882
1983
21970
100 <
100 <
1860
31733
535
7050
100 <
100 <
408
100 <
100 <
100 <
100 <
100 <
100 <
432
5865
100 <
1275
100 <
11634
42390
56351
13137
100 <
100 <
300
100 <
Inject 2
44832
100 <
11888 <
100 <
30702
100 <
537
100 <
1920
2369
22108
100 <
100 <
1798
40474
•'515
6951
100 <
100 <
411
100 <
100 <
100 <
100 <
100 <
100 <
421
5304
100 <
1254
100 <
11406
43533
. 53320
12825
100 <
100 <
296
100 <
Average Deviation Mass (mg)
44104
100
11806
100
31066
100
471
100
1901
2176
22039
100
100
1829
36104
525
7001
100
100
410
100
100
100
100
100
100
427
5585
100
1265
100
11520
42962
54836
12981
100
100
298
100
1.7%
0.0%
0.7%
0.0%
1.2%
0.0%
14.0%
0.0%
1.0%
8.9%
0.3%
0.0%
0.0%
-v1.7%
12.1%
1.9%
0.7%
0.0%
0.0%
0.4%
0.0%
0.0%
0.0%
0.0%
0,0%
0.0%
1.3%
5.0%
0,0%
0.8%
0.0%
1,0%
1.3%
2.8%
1.2%
0.0%
0.0%
0.7%
0,0%
0.30
0.03
0.10
0.03
0.22
0.03
0.04
0.03
0.05
0.05
0.17
0.03
0.03
0.04
0.25
0.04
0.08
0.03
0.03
0.04
0.03
0,03
0,03
0,03
0.03
0.03
0.04
0.07
0.03
0.04
0.03
0.10
0.29
0.36
0.11
0,03
0,03
0.04
0.03
-------
LASCO
Job No. 97-3020
Initial Calibration:
Tube Samples
File: TUBE WK2.WQ2
Standard Curve from 5/19/97
Sfyrene
Purity
Density
Slope
Intcp
AvgRF
99.0%
0.91
288535.9
-1359.5
3.44E-06
Inj. Vol.
Std./Fit
Peak Areas
Avg./Dev.
RF
Low Standard
1.2
1.1
313821
322729.5
3.35E-06
Mid Standard
uL
3.9%
331638
2.8%
6.0
5.4
1559010
1533688
3.5E-06
uL
-1.6%
1508366
1.7%
High Standard
12.0
10.8
3153635
3129031
3.45E-06
uL
0.4%
3104427
0.8%
Blank Avg
0 Note: Average area counts are reagent blank corrected
-------
1
10-
3 9-
•o 8-
a
g 7-
3 6-
t=-
< 4-
t 3-
I
t§ 2-
1-
0-
STYRENE Calibration
3227Z9.5
1533688
Area Counts
3129031
Styrene Calibration
Curve linearity check
Zero
Std1 low
Std2 mid
Std3 high
uL
0
1.2
6
12
Regression Output:
Constant
Std Err of Y Est
R Squared
No. of Observations
Degrees of Freedom
X Coetficient(s) 288700.8
Std Err of Coef. 4288.761
Corrected
0
1.08108
5.4054
10.8108
-2763.61
29567.12
0.999779
3
1
Area count
0
322729.5
1533688
3129031
Corr. Coefficient
0.9998897
-------
LASCO
Job No. 97-3020
Calibration:
Tube Samples
File; TUBE WK2.WQ2
Standard Curve from 5/19/97
Cumene
Purity
Density
Slope
Intcp
AvgRF
Low Standard
99.9%
0.86
311862.7
-34792.2
3.29E-06
Inj. Vol.
Std./Fit
Peak Areas
Avg./Dev.
RF
1.5
1.3
425122
428664.5
3.01 E-06
uL
15.3%
432207
0.8%
Mid Standard
6.0
5.2
1413539
1395503
3.69E-06
uL
-11.0%
1377466
1.3%
High Standard
12.0
10.3
3301385
3261372
3.16E-06
uL
2.5%
3221358
1.2%
Blank Avg
0 Note: Average area counts are reagent blank corrected
-------
11-
10-
^ 9-
| 8-
1 7"
2- 6-
I 5.
•a
I 3-
2-
CUMENE Calibration
428664.5
1395502.5
Area Counts
3261371.5
Cumene Calibration
Curve linearity check
Zero
Stdt low
Std2 mid
Std3 high
uL
0
1.5
6
12
Regression Output:
Constant
Std Err of Y Est
R Squared
No. of Observations
Degrees of Freedom
X Coefficierrt(s) 31 6605.5
Std Err of Coef. 31 425.62
Corrected
0
1.28871
5.15484
10.30968
-72875.5
201138.1
0.990244
3
1
Area count
0
428664.5
1395503
3261372
Corr. Coefficient
0.9951 1
-------
LXISCO Tube Samples Standard Curve from 5/19/97
Job NO. 97-3020 File: TUBE_WK2.WQ2
Calibration:
Methyl Methacrylate Low Standard Mid Standard High Standard
Purity
Density
Slope
Intcp
AvgRF
Blank Avg 0 Note: Average area counts are reagent blank corrected
99.0%
0.94
166066.2
-5619.1
5.83E-06
Inj. Vol.
Std./Fit
Peak Areas
Avg./Dev.
RF
1.2
1.1
235866
237059.5
4.71 E-06
uL
30.9%
238253
0.5%
6.0
5.6
832159
807377.5
6.92E-06
uL
-12.3%
782596
3.1%
12.0
11.2
1925615
1900278
5.88E-06
uL
2.8%
1874940
1.3%
-------
12-
_i 10
1
o
U
MMA Calibration
237059.5
807377.5
Area Counts
1900877.5
Methyl Methacrylate Calibration
Curve linearity check uL
Zero 0
Stdt low 1.2
Std2 mid 6
Std3high 12
Regression Output:
Constant
StdErrofYEst
R Squared
No. of Observations
Degrees of Freedom
X Coefficient(s) 1 66544.2
Std Err of Coef . 1 6488.78
Corrected
0
1.11672
5.5836
11.1672
-2078.49
117422.7
0.990293
3
1
Area count
0
237059.5
807377.5
1900278
Corr. Coefficient
0.995135
-------
LASCO Tube Samples Standard Curve from 5/19/97
' Job NO. 97-3020 File: TUBE_WK2.WQ2
Continuing Calibrations: ;-
Expected
Inject 1 Inject 2 Average Deviation Mass (mg) (mg) Error
Concal "
5/21/97 Styrene 1671766 1639020 1655393 1.0% 5.7 5.9 -3.3%
@ 10:34
Concal
5/21/97 Styrene 1749622 1820856 1785239 2.0% 6.2 5.9 4.2%
@ 18:21
Concal
5/22/97 Styrene 1650673 1760397 1705535 3.2% 5.9 5.9 -0.4%
@2:26
Concal
5/22/97 Styrene 1781913 1813355 1797634 0.9% 6.2 5.9 5.0%
-------
LASCO Tube Samples Standard Cun/e from 5/19/97
Job NO. 97-3020 File: TUBE_WK2.WQ2
Continuing Calibrations:
Expected
Inject 1 Inject 2 Average Deviation Mass (mg) (mg) Error
Concal
5/21/97 Cumene 1531862 1500336 1516099 1.0% 5.0 5.2 -4.4%
@ 10:34
Concal
5/21/97 Cumene 1607211 1675417 1641314 2.1% 5.4 5.2 3.4%
©18:21
Concal
5/22/97 Cumene 1514010 1615963 1564987 3.3% 5.1 5.2 -1.4%
@2:26
Concal
5/22/97 Cumene 1641625 1667710 1654668 0.8% 5.4 5.2 4,2%
@16:35
-------
LASCO Tube Samples Standard Curve from 5/19/97
Job NO. 97-3020 File: TUBE_WK2.WQ2
Continuing Calibrations:
Expected
Inject 1 Inject 2 Average Deviation Mass (mg) (mg) Error
Concal
5/21/97 Methyl Methacrylat 735470 732471 733971 0.2% 4.5 4.8 -7.5%
@ 10:34
Concal
5/21/97 Methyl Methacrylat 757277 787351 772314 1.9% 4.7 4.8 -2.7%
@ 23:30
Concal
5/22/97 Methyl Methacrylat 713704 754327 734016 2.8% 4.5 4.8 -7.2%
@2:26
5/22/97 Methyl Methacrylat 1^7654 170309 17>«J82 2^%
©16:35 ' • S
-------
i LAS CO Tube Samples Standard Curve from 5/19/97
Job NO. 97-3020 File: TUBE_WK2,WQ2
Desorption Efficiency Study; Charcoal - 5/21/97 BHR
Desorp.
Spike Level Efficiency
Inject 1 Inject 2 Average Deviation Mass (mg) (blank corr.)
0 < 100 < 100 100 0.0% 0.01
0.9009 196351 199217 197784 0.7% 0.69 76.6%
4.5045 1053672 1027860 1040766 1.2% 3.61 80.2%
9.009 2104049 2203707 2153878 2.3% 7.47 82.9%
Average 79.9%
-------
Standard Curve from 5/19/97
LASCO Tube Samples
Job NO. 97-3020 File: TUBE_WK2.WQ2
Desorption Efficiency Study; Charcoal - 5/21/97 BHR
Desorp.
Spike Level
(mg)
0
0.86
4.3
8.6
Inject 1
< 100 <
247201
1200100
2313958
Inject 2
100
250869
1173132
2420783
2859174
Average
10
249035
1186616
2367371
Deviation
900.0%
0.7%
1.1%
2.3%
Mass (mg)
0.11
0.91
3.92
7.70
Average
Efficiency
(blank corr
105.8%
91.1%
89.6%
95.5%
-------
LASCO Tube Samples Standard Curve from 5/19/97
Job NO. 97-3020 File: TUBE_WK2.WQ2
Desorption Efficiency Study; Charcoal - 5/21/97 BHR
Desorp.
Spike Level Efficiency
(mg) Inject 1 Inject 2 Average Deviation Mass (mg) (blank corr.)
0 < 100 < 100 100 0.0% 0.03
0.9306 93793 95070 94432 0.7% 0.60 64.7%
4.653 552721 538699 545710 1.3% 3.32 71.4%
9.306 1117140 1175094 1146117 2.5% 6.94 74.5%
Average 70.2%
-------
APPENDIX B.2
Method 18 GC Chromatograms
-------
rw-«-<-«*/ P-0-BOX4159
D66CO™ Gary, NC 27519
1-800-733-3261 Fax (919) 250-1835
Lasco, Inc. / PES
GC Chromatograms
& M25A Recorder Traces
-------
pi: 11 :8897/85/15
r 1-908
4.825
5. £75
9.656
CHROMATOGRAfl 1 MEMORIZED
CR5B1 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO B
REPORT HO 95
PKMO
LASCO TUBES
FILE
METHOD
TIME
1.908
4.825
5.275
9.656
TOTAL
AREA MK IDNO COHC
e
8802
€
U
377 3
202427
136Q
888
£13369
4
1
NAME
99.6824 CSS
EL 39/6 STYREME
180
-------
38:51:0997/85/15
— 1.908
4.82!
5. £73
6. £ 6 2
9.655
CHROI1ATOGRAM 1 MEMORIZED
CR5Q1 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO O
REPORT HO 94
PKNO
TIME
1
£
3
4
5
1.903
4.025
5.273
6.262
9.655
992£
218254
1526
311
1166
TOTAL
231118
LASCO TUBES
FILE
METHOD
0
0002
AREA MK IDHO
COHC NAME
99.496 CS2
0.504 STYRENE
186
o
o
-------
Jl:31:0697/95/15
LASCO TUBES
1.915
5. £75
6.261
4 fi^
T • V v1 i
9.6
CHRGtIATOGRAII
1
MEMORIZ
ED
CR581 CHROHATOPflC
CHANNEL- HO 1
SAHPLE HO 0
REPORT HO 96
PKNO
TIME
TOTAL'
AREA Ml< IDHO
1
2
3
4
5
1.915
4.833
5.275
6.261
9.655
2385
£94359
419
282
442
207887
FILE
METHOD
COHC
HAI1E
99.7842 CS£
3.2153 STYRENE
100
-------
D1S51
• 1.
5.
6.
9.
:0397/05/
912
£67
£62
65
15
fl OO
U OO
LASCO TUBES
rJHROMATOGRAII 1 MEMORIZED
CR5Q1 CHROI1ATOPAC
CHANNEL HO 1
SA11 RLE HO 3
REPORT NO 97
PKHO
1
2
•j
4
5
TIME
1.912
4.833
5.267
6.262
9.65
AREA
2355
204422
''421
280
259
MK IDNQ
FILE
METHOD
CONC
0
0002
HHflE
99.6734 CSS
3.1266 STYREHE
TOTAL
297737
180
-------
J2: 11:6297/95/1 5
1:181
3.029
•r — ~*~— **-
5.274
6.26
V • .• U L.
10.136"""
CHROHATQGRAH 1
CR5Q1
CHROtlflTOPAC
4.Q32
MEMORIZED
CHANNEL HO 1
SAMPLE
REPORT
PKNO
1
£
3
4
5
6
7
8
9
10
11
HO 0
MO,. 98
TIME
1.597
1.968
3.029
4.032
5.274
6.26
6.922
9.307
9.4QS
9.652
10.136
AREA MK
1282
949
22367
£04827
426
286
144936
654
2293 '•/
729939
1087
LASCO TUBES tf~
FILE 9
METHOD 8992
IDHO CONC NAME
4 18.8917 CS2
3 13.4203 flttft
1 67.5874 STYREHE
2 8. 1006 CUHEME
TOTAL
1188229
-------
32:31:9497/65/15
!:§!§
LASCO TUBES
3.03
4 Ci •:• '•
.000
5.273
6.259
10.125 "
CHROMATOGRAM 1 MEMORIZED
CR561 CHROMATOPAC
CHAMMEL HO 1.
SAMPLE HO 0
REPORT HO 99
10
10
I
6
to
>KMQ
TIME
AREA MK I DUO
FILE
METHOD
COMC
MflHE
1
c
3
4
5
6
7
8
9
10
11
1.598
1.918
3.93
4.633
5.273
6.259
6.921
9.3B5
9.497
9.651
19.125
1253
918
£2061
2B3994
424
292
146550
675
2347
745980
1136
1
p
18.5844 CS2
13.3512 t1MA
67.9609 STYRENE
8.1Q35 CUHEHE
TOTAL
1125629
168
-------
Q£:5150297/05/15
j- 1.9G8
4.831
5.£7
6. £59
CHROMATOGRAtt 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO B
REPORT HO 100
PKMO
1
£
3
4
TIME
1.908
4.831
5. £7
6.259
AREA
4949
£14406
14 £7
£85
TOTAL
£21067
LASCO TUBES
FILE
METHOD
CONC
100
100
0
0002
HA ME
-------
D3:11:9197/95/15
LHStU IUBLB
- '1.908
5.258
4.02S
CHRQHATQGRAfl 1 MEMORIZED
CR5Q1 CHROI1ATOPAC
CHANNEL NO 1
SAMPLE HO O
REPORT NO 181
1
PKNO
1
2
3
TIHE
1.998
4.B2S
5.253
AREA MK IDHO
4286 '
187804 4
1287
FILE
METHOD
COHC
109
8
OG02
HA ME
CSS
TOTAL
193213
180
-------
D3:38:5997/05/15
LASCO TUBES
1.91
5.£69
I-3A
4.Q29
CHROtlATOGRAM 1 MEMORIZED
CR5Q1 CHROI1ATOPAC
CHANNEL HO 1
SAMPLE HO 9
REPORT HO 102
FILE
METHOD
8
G0B2
PKHO
1
2
3
TIME
1.91
4.029
5.269
TOTAL
AREA MK IDHO
2323
137131 4
429
139883
CONC
180
109
HAHE
CS2
-------
93:50:5597/05/15
1.91
4.03
5.2?
6. £57
CHROMATOGRACI 1 MEMORIZED
CR5Q1 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 9
REPORT NO 103
PKNO
-..•-.' 1
£
LASCO TUBES
TIME
1.91
4.03
5.27
"6. £57
TOTAL
AREA ,1K IDNO
£598
SB 1871 4
480
£
S95E21
FILE
METHOD
COHC
100
100
0
0062
NAME
csa
la
-------
34:19:5297/05/15
4.0£!
5.264
6. £53
9.649
CHROHATOGRAH 1 MEMORIZED
CR501 CHROMATOPAC
CHAMMEL NO 1
SAMPLE NO 8
REPORT' NO 104
PKMO
TIME
1
2
3
4
5
1.399
4.025
5.264
6.253
9.649
52237
197281
1164
£68
519
LASCO TUBES
AREA UK IDNO
FILE
METHOD
CONC
NAME
Q Q 7 -~> ~? o r-
-• -• • / -ji o L
9.2622 STYRENE
TOTAL
251498
100
-------
J4:38:4697/85/l5
LASCO TUBES
4.833
1.904
5.£73
6.£61
9.656
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHANNEL HO 1
SAMPLE MO 9
REPORT MO 105
PKMQ
TIME
AREA M!< I HMO
FILE
METHOD
COHC
8
B00£
1
2
3
4
5
1.904
4.033
5.273
6.261
9.656
TOTAL
5039G
191917
1052
£53
535
244147
4 99.
1 8.
100
722
£73
NAME
CS2
o
o
•o
I
-------
14:58:4497/65/15
1.911
5.271
4.Q29
9.653
CHROMATOGRAM 1 MEMORIZED
CR5Q1 CHROtlATOPAC
CHAHNEL HO 1
SAMPLE MO 8
REPORT MO 106
KMO
TIME
LASCO TUBES
6
I
Nl
6
NJ
TOTAL
AREA MK IDHO
FILE
METHOD
COUC
0
000E
192688
HA ME
1
2
3
4
1.912
4.G29
5. £71
9.653
766 ••,
190S40
345
1337
4
1
99.3D££
0.6978
100
-------
35:19:3997/95/15
1.312
4.024
5.265
9.647
CHROMATOGRAI1 1 MEMORIZED
CR591 CHROMATQPAC
CHANNEL HO 1
SAMPLE HO 9
REPORT HO 107
LASCO TUBES
FILE
METHOD
9
9092
PKNQ
... .1
is
"3
4
TIME
1.912
4.924
5.265
9.647
AREA 11 K
737
1881 11
336
1339
IDHO CONC
4 99.
1 0.
£981
7919
TOTAL
199514
HAI1E
190
-------
35:38:3597/95/15
1.91
5.262
4.026
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHAHMEL HO 1
SAMPLE HO Q
REPORT HO 108
LASCO TUBES
PKHO
TIME
1.91
4.026
5. £62
TOTAL
AREA MK I UNO
£931
186459 4
£523
FILE
METHOD
CQMC
9
0002
HAME
cs
Op
oc
191919
100
o
o
N)
to
u>
©
-------
(35: 58: £897/85/1:
1.911
5. £69
6. £6
4.03£
CHROMATOGRAH 1 MEMORIZED
LASCO TUBES
CHROMATOPAC
CHANNEL MO 1
SAMPLE NO. 0'
REPORT NO 109
PKNO
TIME
TOTAL
AREA f1l( i DM0
1
£
3
4
1.911
4.03£
5.269
6. £6
3464
£06196
2964
£88
£1£85Q
TILE
METHOD
CONC
100
100
Q
08 0£
NAME
CSS
-------
96:16:2397/85/15
LASCO TUBES
1.9B7
i.258
4.827
CHROI1ATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE. NO B
REPORT HO 11Q
PKHO TIME AREA MK IDNO
1 1.997 1346
£ -4.827 189110 4
3- 5.258 669
FILE
METHOD
COMC
1QB
B
0002
NAME
CS2
s>
ro
U>
6
K)
o
01
TOTAL
191625
100
-------
36:30:1497/85/15
1,906
4.025
5.266
CHROHATQGRAH 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO I
SAMPLE -HO 0
REPORT HO 111
LASCO TUBES
PKNO
TIHE
1.996
AREA UK IDHO
1798
FILE
METHOD
COHC
0
8002
HAtlE
£
3
4.025
5.£66
TOTAL
188038
662
196490
190
CS2
180
-------
116:50:8797/05/15
4.823
LASCO TUBES
5.264
6.249
9.641
CHROMATQGRAM 1 MEMORIZED
CR581 CHROnATOPAC
CHANNEL HO 1
SAMPLE MO O
REPORT HO 112
PKHO
1
2
3
4
5
6
7
8
9
10
11
.12
13
14
TIME
AREA MK IDM0
FILE
METHOD
COMC
8082
NAME
1.59
1.987
3.014
4.0E3
5.264
6.249
6.913
9.299
9.461
9.641
18.129
18.441
10.541
1Q.849
574
1414
45688
193G53
1038
263
326657
18483
64203 V
4394997 VE
5858 V
2719 V
295 V
930
1
2
3.562 CSS
15.2527 MMA
81.0921 STYREHE
9.8932 CUMEHE
KJ
10
U
6
to
o
u
VI
6
to
TOTAL
5555192
188
IQ
-------
37:99:5997/05/15
LASCO TUBES
4.624
5.£58
6.£53
9.641
CHROMATOGRAH 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL 110 1
SAMPLE NO 8
REPORT NO 113
FILE
METHOD
0
80Q2
PKMO
TIME
AREA UK IDM0
COHC
NAME
1
2
3
4
5
6
10
11
12
13
14
1.594
1.911
3.013
4.824
5.258
6.253
6.917
9.3Q3
9.486
9.641
16.135
18.448
18.55
10.857
557
1357
43251
185731
971
£47
773904
17224
61135 V
4322457 VE
49£0 V
£51 £ V
366 V
867
•~t C * *"» f" 0 *"*
o • M o Use
14.6378 (IMA
81.7561 STYREME
Q.0931 CUMEME
TOTAL
5415498
186
-------
37:29:5597/05/15
LASCO TUBES
1.909
5.265
•I*
4,827
9.647
CHROHATOGRPfl 1 MEMORIZED
CR5B1
CHANNEL
SAMPLE
'REPORT
F'KNO
1 •
/•,
c
3
4
CHROMATOPAC
HO 1
HO Q
HO 114
TIME
1.989
4.027
5.265
9.647
AREA UK
1237
289227
892
1490
ID NO
4
1
TOTAL
FILE
METHOD
COHC
0
0GQ2
NAME
203845
99.2616 CSS
8.7384 STYREHE
100
CJ
ro
10
CJ
6
Is)
O
LJ
VI
6
NJ
If
-------
07:49:4897/85/15
1.913
5.253
4.031
CHROflATOGRAM 1 MEMORIZED
CR5Q1 CHROHATOPAC
CHANNEL NO 1
SAMPLE NO 0
LASCO TUBES
FILE
METHOD
9
0002
REPO;RT
'•i ' '!"•
PKNO ".*'
1
2
3
4
HO 115
TIME
1.913
4.031
5.258
9.652
T r. T A i
AREA MK
1182
136952
860
753
IDNO
4
1
COMC
99.
0.
6189
3811
19974?
NAME
.3811 STV
180
-------
38:99:4697/65/15
LASCO TUBES
4.026
5.266
3. aias
CHRQMATOGRAH 1 MEMORIZED
CR5Q1 CHROHftTOPftC
CHANNEL HO 1
SAMPLE'HO 8
REPORT HO 116
KHO
TIME
TOTAL
AREA MK
1750269
:DHO
TILE
METHOD
COHC
0
0082
HA HE
1
£
3
4
5
6
7
8
9
18
11
1.592
1.91
3.917
4.8£6
5. £66
6.919
9.385
9. 486
9.651
10.125
10.45
1681
1878
51724
197578
1895
259497
977
3546
1230518
2259
414
V
V
V
2
11.6917 CSS
15.3563 MMA
72.81 S3 STYREHE
8. 1337 CUflEME
100
-------
J8:£9:4297/95/15
LASCO TUBES
4.825
5.264
CHROMATQGRAtl 1 MERQRIZED
CR581 CHRDMATOPAC
CHANNEL HO 1
SAMPLE HO Q
FILE
METHOD
G
Q082
REPORT HO 117
PKMO
TII1E
TOTAL
AREA MK IDHO
1
2
3
4
5
6
7
8
9
IB
11
1.594
1.312
3,018
4. Q25
5.264
6.917
9.385
9.487
9.652
19.136
18.455
1518
1813
49007
188254
1039
246858
906
3245
1168310
1864
385
V
V
166E400
1
2
COMC
NAME
11.7271 CS2
15.3778 MMA
72.7789 STYRENE
0.1161 CUHEHE
100
-------
1:4097/05/15
LASCO TUBES
1.908
4.03
6.259
C.C'DD
CHROMATQGRAI1 1 MEMORIZED
CR501 CHROttATOPAC
CHAMHEL HO 1
SAOPLE NO 8
REPORT HO 118
PKNO
TIME
TOTAL
AREA UK I DUO
FILE
METHOD
COHC
9
Oboe
eee
10917
MAtlE
1
£,
3
4
5
6
1.
4.
6.
6.
9.
10.
998
83
£59
923
654
137
2885
196528
383
177144
384658
338319 V
4
O
1
2
IB.
16.
35.
OQ
w 0 .
0525
£719
3335
3421
CS2
MM A
3TYRENE
CUI1EI1E
KJ
o
faj
100
-------
57/85/15 12:20:0
CR581 CHRQMATOPAC
CHANNEL NO £
SAMPLE NO G
REPORT NO 113
PKMO TIME AREA
1 2.49 19131
2 £.583 62793
7 LftSCO BAG SAMPLES
!
FILE 9
METHOD seas
(1K IDNO CONC NAME
1 83.3526 METHANE
V 2 76.6474 ETHANE
TOTAL
81924
189
-------
12:28:5897/95/15
1.911
4.033
6. £62
LflSCO TUBES
CHROHATOGRAtt 1 MEMORIZED
CR5Q1
CHAMMEL
SAMPLE
REPORT
PKHO
1
£
3
4
5
6
CHROMATOPAC
HO 1
HO 3
HO 1£0
TIME
1.911
4.933
6. £62
6.9£5
9.656
19.138
TOTAL
AREA UK
2605
192314
£53
173999
331343
329017
1079530
I DM0
4
3
1
£
FILE ,
METHOD
COHC
17.
16.
^ ^
o o .
30.
10B
0
OQG£
NAME
S619 CS£
1608 Mtlfi
4137 STYRENE
5587 CUMEME
(O
KJ
u
6
KJ
O
CJ
-------
57/65/15 12:4Q:18
LASCO BAG SAMPLES
§1*83
CR581 CHROHATOPAC
CHANNEL HO 2
SAMPLE HO 8
REPORT HO 1S1
FILE
METHOD
9
Q80S
PKI10
1
2'
TIME
2.49
2.58
AREA MK IDNO
18669
61328 V
i
£
CONG
NAME
23.3399 METHANE
76.6601 ETHANE
TOTAL
79989
108
-------
1 C i T o i vi O ? /• '
3.^42
5. £67
6.263
6.93
'- 9.657
CHROMATOGRAM 1
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO O
REPORT NO 122
PKMO TIME
1 1.397
2 1.599
3 1.913
•4 £.165
5 3.042
6 3.47
7 4.033
8 5. £67
9 6.263
10 6.93
11 9.657
V
-------
LASCO BAG SAMPLES
2.785
U>J0
1.491
CR581 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO 8
REPORT HO 183
PKMO
1
2
TIME
2.491
£.581
2.785
AREA !1K IDHO
31605 1
1879 V £
367 V
FILE
METHOD
CONC
Q
6888
NflHE
94.3886 METHANE
5.6113 ETHAHE
TOTAL
33858
168
-------
13:08:5997/05/15
• 1 SQ3
i •«?§
* . 52 3
c. • 1 D C
LASCO TUBES
4.035
5. £67
6.£62
6.927
r 5.653
CHROI1ATOGRAH l MEMORIZED
CR501 CHROflATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT NO 124
PKMO
1
£'
3
4
5
6
7
8
9
18
11
TIME
AREA MK IDM0
1.393
1.595
1.9
2. 168
3.84S
3.471
4.035
5. £67
6. £62
6.9£7
9.653
355
4045
1556
1252
1445
503
£19018
1131
433
847
6266
FILE
METHOD
CDNC
0
8662
NAME
96.3544 CS£
0-3745
STYRENE
o
CO
TOTAL
236895
180
-------
97/85/15
13:20:33
LASCQ BAG SAMPLES
of*'
\0
*
2.49
CR5B1 CHROflATOPAC
CHANNEL NO 2
SAMPLE NO 8
REPORT NO 125
PKNO
1
'£
o
TINE
2.49
£.58
2,784
AREA
31923
1893
377
H
V
V
IDHO
FILE
METHOD
CONC
94.492
5.598
9
9082
NAME
METHANE
ETHANE
TOTAL
34194
198
-------
\- 1.912
5.27
6.259
4.025
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHftMMEL NO 1
SAMPLE NO 9
REPORT HO 126
PKHO
TIME
AREA UK IBNO
FILE
METHOD
COHC
0
GODS
NAME
1
ft
3
4
1.912
4.GE5
5. 2?
6.259
6131
219772
££79
312
TOTAL
£28494
109
100
CS2
-------
?7/85/14 15:48:5?
F 27? 9
LflSCO BAG SAMPLES
2.496
CR5B1 CHRQMATOPAC
CHANNEL HO 2
SAMPLE HO 8
REPORT HO 41
PKNO
1
^.
c
•-T
o
TIME
. a. 496
2.58?
2.79
AREA
33994
1914
411
n
V
V
TOTAL
IDMO
FILE
METHOD
COHC
9
8882
HAME
94.6566 METHANE
5.3434 ETHANE
180
-------
15:50:1297/85/14
LASCQ TUBES
1.988
4.03?
6. £69
I ig:S?i
CHRQI1ATOGRAH 1
MEMORIZED
CR501 CHRQHATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT NO 4£
PKNQ TIME
1 1.968
2 4.83?
3 6.269
4 6.931
5 9.664 1
6 18.148 2
7 18.542
8 18.872
AREA
824
186628
278
914954
867256
317357
2612
£61
HK IDHO
FILE
METHOD
CONC
8
0882
W
to
6
8
CO
NAME
TOTAL
529815;
3.5383 CS2
17.3084 MMA
35.3233 STYREME
43.838 CUMEI1E
100
-------
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
2
3 .
37/85/14 16:81:42 LASCO BAG SAMPLES
CHROMATOPAC
NO 2 FILE 9
HO B METHOD G982
HO 43
TIME AREA MK IDNO COHC NAI1E
2.496 34934 1 94.6631 METHANE
2. 536 1970 V 2 5.3369 ETHANE
2.789 422 V
TOTAL 37325 180
2.496
-------
6:10:4497/05/14
LASCO TUBES
1.924
4.839
6. £72
U. J04
m?
CHROMflTOGRfltl 1 MEMORIZED
CR501 CHROnftTOPAC
CHAMMEL NO 1
SAMPLE HO 0
REPORT MO 44
PKMO
TIME
AREA UK IDHO
FILE
METHOD
COHC
G
0002
MA HE
1
£
3
4
5
6
1.924
4.039
6.272
6.934
9.317
9.666
19. 155
10.565
19.707
623
£02512
300
540734
535
1048067
1413161
2162
3371
V
1
2
TOTAL
3211464
6.3197 CSE
16.8743 llflfl
32.7D64 STYRENE
44.0996 CUHEHE
180
-------
S7/85/1
LASCO BAG SAMPLES
--.<-, il . OOO
£.496
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE HO O
REPORT HO 45
FILE
METHOD
9
0002
PKNO
TIME
AREA UK I UNO
COHC
HAtlE
1
£ •
3
2.496
£.586
£.79
33165
187£
395
TOTAL
94.6565 METHANE
5.3435 ETHANE
3543£
100
-------
£ • "37 • P
t>: J/ : Db^/'
1.998
===••—
6. £69
' 0 3 / 1 ^
4.033
LHbl
JU IHiiLb
'-' . .•' w L.
1
1 }§:?*§
CHROMATOGRAM 1
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
£
3
4
5
6
7
8
-• • 'J \J «j ,
A W • i
MEMORIZED
3HROMAT rj UA
HO 1
HO 0
HO 46
TIME
1.908
4.G33
6. £69
6.93E
9.665
19.15
10.542
18.785
^
AREA MK
569
189456
£66
478995
993904
1214978
3 £7
3860 V
FILE 0
METHOD 0002
IDNO CQNC NAME
4 6.797 CS£
3 17.1847 I1MA
1 32.429 STYRENE
£ 43.5893 CUtlEHE
TOTAL
£792353
108
-------
37/05/14 16:49:26
LASCO BAG SAMPLES
to
KO
W
6
8
<»4
6
CR5B1 CHROHATOPAC
CHANNEL NO E
SAHPLE NO 8
REPORT HO 47
FILE
METHOD
9
9882
PKNO
1
2
3
TIME
2.498
£.589
2.791
AREA MIC I DUO
114561
. 4668
1864
CONC
NAME
1
I
96.9851 METHANE
3.9149 ETHANE
e
TOTflL
120S93
188
-------
58:3897/95/14
1.924
4.843
6. £76
CHROMATOGRAM
1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL MO 1
SAMPLE MO 9
REPORT HO 48
PKNO
TIME
LASCO TUBES
TOTAL
AREA UK IDHO
FILE
METHOD
CONC
0
9BO£
1
c
3
4
5
HI ,32 4
4.043
6. £76
9.383
9.798
'?!£
£19193 4
-;*. 3£4
3017
9332 V
100
£32773
HA ME
CS£
100
-------
£.792
LASCO BAG SAMPLES
1.498
CR581 CHROHftTOPAC
CHANNEL NO 2
SAMPLE HO 9
REPORT NO 49
FILE
METHOD
9
eeee
PKHO
c
3
TIME
2.498
E.59
2.792
AREA UK IDNO
119768 1
4879 V £
1167 V
.p.
CONG
HftflE
96.Q926 METHANE
3.9@74 ETHANE
TOTAL
125745
189
-------
CHROI1ATI
1/:2B:5997/
1.922
-
6.277
3GRAM 1
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 8
REPORT HO 58
PKNO TIME
. 1 1.922
2 4.033
3 6.277
TOTAL
05/14 LASCO TUBES 2$?^
6
K>
9WF
. 10.A*
: |
MEMORIZED ' P
FILE n
t A ^ W \_l
METHOD 0002
AREA t1K I DM0 COHC MAHE
S44
286421 4 100 CS2
298
207563 i0g
1
i
-------
97/95/14 17:32:19
LASCO BAG SAMPLES
id
a.49?
CR581 CHROtlATOPAC
CHANNEL MO 2
SAMPLE NO 8
REPORT MO 51
PKNO
1
2
3-
TItlE
2.497
£.587
2.791
AREA m< IDHO
32246
1B59 V
2851 V
1
£
FILE
METHOD
CONC
9
Q882
NflHE
94.5737 METHANE
5.4263 ETHANE
TOTAL
J6148
198
-------
r 1:!?!
4.043
6. £8
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT HO 5S
FILE
METHOD
v<
F
Q
0002
PKHO
TIME
TOTAL
AREA MK I UNO
1
,— ,
c
3
4
1.399
1.918
4.043
6. £3
199
5013
£16648
•' 317
£££169
CONC
180
100
NAME
• CO
• oc
-------
17:53:£8
LftSCO BAG SAHPLES
2.498
C . f 5.
CR581 CHROMATOPAC
CHANNEL NO 2
SAMPLE HO 9
REPORT NO 53
PKNO
1
£
3
TIME
TOTAL
AREA UK IBNO
FILE
METHOD
CONC
9
8882
2.498
£.589
2.793
32887
1848
2885
V
V
1
£
36748
NAME
94.6662 METHANE
5.3338 ETHANE
186
-------
18:0£:5197/05/14
LASCO TUBES
3.071
5. £95
6.279
6.945
4.846
CHROMATOGRAtt
CR501 CHRQMATOPAC
CHANNEL HO 1
SAMPLE MO 8
REPORT MO 54
MEMORIZED
PKNO
TIME
IIK IDNO
FILE
METHOD
COMC
0
OOG2
MA HE
1
£
3
4
5
7
3
9
10
1.399
1.601
1.919
£.17
3.071
4.046
5. £95
6. £79
6.945
9.67£
T ft T A I
494
3034
3£85
867 V
483
£01693
341
437
321
5654
:-
4 97.1££8 CS£
3 0.1544 MMA
1 2.7££8 STY
£16609
(0-jl
it
J
l
100
-------
(18:83:3797/05/14
LASCO TUBES
h. •
^ n?
3.074
5.294
6.267
6.933
r 9.666
4. 946
CHROMATOGRAH 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
2
3
4
5
6
7
8
9
10
CHROMATOPAC
HO 1
NO 0
HO 56
TIME
1.403
1.6S5
1.922
£. 174
3.074
4.046 21
5.294
6.267
6.933
9.666
AREA
555
3427
3782
978
539
8955
397
498
362
6434
DUO
FILE
METHOD
COMC
0
8302
NAME
96.9893 CSS
8. 1604 MMA
2.8502 STYRENE
TOTAL
£35848
100
-------
8:44:2197/65/14
LASCO TUBES
v
1.916
c
i
4..637
CHROtlATOGRAM 1 MEMORIZED
CR581 CHRGMATOPAC
CHANNEL HO 1
SAHP1E HO B
REPORT HO 58
FILE
METHOD
G
8902
PKNO
v. 1
C
-;' 3
4
5
TIME
L.,9.16
4 . 8f 7 .
6Q *? 1 ••'
• 7 ^J.-'i " • *•
9.665""
10.152
AREA
3566
164246
169927
\361653
311554
t1K IDNO
o
1
2
CONC
NAME
17.9336 CSS
16.5399 UNA
35.2815 STYREME
38.3251 CUMEME
TOTAL
183B939
188
..a
-------
1.918
4.643
CHROtlATOGRAM 1 MEMORIZED
CR5G1 CHROMATOPAC
CHftHMEL HO 1
SfltlPLE HO B
REPORT HO 60
PKMO
1
O
3
4
5
TIME
1.918
4.043
6.937
9.668
10.153
3522
184481
171239
368725
316622
AREA 11K IDHO
4
2
1
£
FILE
METHOD
COHC
G
0802
17.7283
16.4434
418
413S
35
38
NAME
CS2
MMft
STYREHE
CUMEME
TOTAL
1044589
100
-------
1 ? t CD • OU ?/ '
i . 3 I
5.275
6.274
9.658
CHROMATOGRAH 1
CR5B1 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 0
REPORT NO 62
PKNO TIME
1
2
3
4
5
1.91
4.043
5. £75
6.274
9.653
TOTAL
C'j/lt LH&LUIUtfLS
4.G43
MEMORIZED
FILE 9
METHOD 9902
AREA MK IBNO COHC HA
73354
292315 4 99.3723 CS2
1229
239
259 1 9. 1277 STY
277447 ififl
-------
97/05/14
19i37:S3
LASCQ BAG SAMPLES
£.794
2.499
CR581 CHROtlATOPAC
CHANNEL HO 2
SAI1PLE HO 8
REPORT NO 63
F'KNO
TIME
TOTAL
AREA I1K IDHO
FILE
METHOD
COHC
9
9882
118188
NAME
1
,2
3
2.
2.
""*
C •
499
592
794
11
2227
4613
1268
V
V
1
£
96.
3.
9516
9484
1@Q
-------
r r 1 ^ /•
1.921
4.Q4I
6. £76
CHROMATOGRAM
1 flEMORIZED
CR5Q1 CHROMATOPAC
CHflMNEL HO 1
SAMPLE HO 8
REPORT HO 64
PKNO
1
2
TIME
1.921
4.G46
AREA
3371
LASCO TUBES
IDHO
FILE
METHOD
COMC
0
0002
NAME
CSS
6.276
TOTAL
324
£21443
100
-------
97/85/14
19:58:04
LASCO BAG SAMPLES
£.733
!.498
CR501 CHROHATOPAC
CHANHEL HO 2
SAI1PLE HO 0
REPORT NO 65
PKNO
TIME
TOTAL
AREA t1K IDHO
FILE
METHOD
COHC
126368
MAflE
1
£
3
2.498
2.591
2.7.93
120588
4923
1358
V
V
1
E
96.6776
3.9E24
100
I
-------
1.922
4.648
6.£8
CHROMATOGRAM 1 MEHORIZED
CR501 CHROdflTOPAC
CHAMNEL 110 1
SAMPLE NO 0
REPORT MO 66
PKNO
1
o
TIME
1.922
4.048
6.23
TOTAL
fiREA f1K IDNO
3266
£1151?
319
£15093
FILE
METHOD
CONC
100
160
0
0002
NAME
CS2
-------
7 ( ' 0 3 f 1
CR581
CHANNEL
SAHPLE
REPORT
«t dOSlS.^J LH5L.U CHU SsHnrLtb _ A
^J^ A
CHROMATOPAC
NO 2
NO Q
NO 67
FILE 9
METHOD 8882
PKNO
1
2
TIHE
2.498
2.59
TOTAL
AREA MK IDNO
17271 1
57819 V £
74298
COHC
NAtlE
23.2481 METHANE
76.7519 ETHANE
108
K:
u:
t>
-------
4.Q47
4.963
6.279
6.946
9.671
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHRQHATOPAC
CHAMNEL HO 1
SAMPLE NO 0
REPORT HO 68
PKHO
TIME
AREA UK IDNO
TILE
METHOD
COHC
NAME
1
2
3
4
5
6
7
1.662
1.923
4.947
4.983
6.279
6.9,46
9.671
1155
1161
20.2099
345
292
OO7
iJ O (
3955
TOTAL
269344
O 7 Q O Ci e, r 1-v O
7 I . 7 C. 0 •-! U -j u
B.I 631 MMA
1.9163 STYRENE
1 QCl
-------
CR5B1 CHROMATOPAC
CHANNEL NO 2
SAMPLE NO 8
REPORT NO 69
PKNO
1
2
TIME
2.498
2.592
AREA MK IBNQ
18551
61699 V
2
FILE
METHOD
COHC
9
008£
MAHE
23.2986 METHANE
76.7094 ETHANE
TOTAL
79650
180
-------
^•'48:4197/85/14
LASCO TUBES
4.899
6.276
6.943
9.669
CHROMATOGRAM
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 0
NO 70
4.033
x\
MEMORIZED
PKNO
TIME
MK IDNO
FILE
METHOD
COHC
£87268
NAME
1
3
4
•
6
7
1.599
1.92
4.033
4.899
6.276
6.943
9.669
T ri T A i
1135
1153
288879
345
283
oo *••
u u C
3942
4
1
97.9082 CS2
0.1626 MMA
1.9292 STYI
100
-------
97/05/1
'1:00:08
£.498
CR591 CHROHATOPAC
CHANNEL NO £
SAMPLE NO 0
NO 71
FKNO
LASCO BAG SAMPLES
\r\
2.498
TOTAL
MK IDNO
677
677
FILE
METHOD
COHC
100
80G£
NAME
METHANE
(,0
-------
: 1697/85/14
923
4.039
6.27
LASCO TUBES
CHRQHATQGRftfl 1 HEHORIZED
CR561 CHRDHATQPAC
CHANNEL NO 1
SAMPLE HO 8
REPORT NO 72
FILE
METHOD
0
08SS
PKHO
1
2
3
4
5
6
TIME
1.923
4.839
6.27
6.933
9.665
10.152
AREA UK
673
194553
271
64378
185442
267858
i UNO
4
"3
1
e
COMC
£7.
9.
26.
o 7
V1 1 *
3166
038
0373
6B81
NAHE
CS2
tin A
STYRENE
CUHEHE
»
I
TOTAL
713158
108
-------
(97/85/14 £1:20:38
£.791
LASCO BAG SAMPLES
N
t~
x.
c
K.
CR581 CHROHATOPAC
CHANNEL MO 2
SAMPLE HO 0
REPORT HO 73
PKNO
TIME
AREA . t1K IDHO
FILE
METHOD
CONG
9
9882
HAME
e
U
1
£
2.497
2.59
3. 791
27032
43565 V
£12 V
1
2
38.2993 METHANE
61.7897 ETHANE
TOTAL
78809
180
-------
CHRQUAT
21:29:3597/85/14
1.921
,"
V • -• •-' V
i .-. .• .- .-
1 -•' J V '-'i*
| 1 U • 1 >J
OGRAH 1
CR501 CHROHATOPAC
CHANNEL NO 1
SfthPLE HO 0
REPORT HO 74
F'KHO TIME
1
£
. 3
4
5
1.921
4.041
6.936
9. 666
18. 15
TOTAL
4.041
MEMORIZED
AREA 11 K
637,
18866Q
61140
176639
£53391
680467
LASCO TUBES
FILE 0
METHOD 8082
I UNO CDNC NAME
4 £7.7511 CSS •
3 8.9934 firifl
1 £5. 98£8 STYRENE
£ 37.2727 CUMEME
108
-------
97/05/14
2U40;58
£.783
LASCO BAG SAMPLES
CR581 CHROHATOPAC
CHANNEL NO 2
SAHPLE 110
REPORT MO
fl
75
PKNQ
1
2
'• o
TIME
2.498
£.59
£.783
TOTAL
AREA UK I UNO
£7177
43800 V-
Z19 V
71196
FILE
METHOD
COMC
9
8002
NAME
Oi
XI
38.£899 METHANE
61.7101 ETHAME
106
(.*
-------
£1:4985597/05/14
1.92
4.043
6.271
i
HENORIZED
CHROHftTOPAC
CHfiMMEL MO l
LfiSCO TUBES
SAMPLI
REPOR-
PKNO
"i
c.
3
E NO o
I" NO 76
TIME
1.92
4.043
6.271
7 n T ft 1
1 u 1 H L
AREA
3258
220265
319
223833
FILE
METHOD
IK IDHO COHC
* 180
— — — —
100
0
0002
HA ME
CS2
-------
i-HHPLi
REPOR;
PKNO
i
E NO o
r NO 7?
TI/1E
2.495
TOTAL
TILE
IDNO
624
CONC
188
9
8802
MflME
-------
1BM397/85/U
1.913
6.268
CJ581 CHROrtflTOPflC
CHANNEL HO 1
SAMPLE NO G
4.637
r< c. r U K 1
PKNO
1
2
•-V
0
NO 78
T I ME
1.913
4.837
6.268
AREA
£499
189883
£56
MIC IBNO
TOTAL
LASCO TUBES
192558
FILE
METHOD
CONC
160
190
0
0982
01
01
8
6
NJ
NAME
CSS
-------
LASCO BAG SAMPLES
'^.738
2.491
CR501 CHROttATOPAC
CHANNEL HO 2
SAMPLE NO 8
REPORT NO 79
FILE
METHOD
9
6802
PKNO
TIME
AREA !1l( IDNO
CONC
HAHE
1
2
3
£.494
£.585
£.783
£9265
1717
£438
1
2
94.4575 METHANE
5.5425 ETHANE
TOTAL
108
-------
iC.00.013/-
*• • A 0 C
1:814
5.282
6.266
9.664
CHROHATOGRAM 1
CR501 CHROflATOPAC
CHANNEL NO 1
SAMPLE NO g
REPORT NO 80
PKNO TIME
1 1.394
£ 1.596
3 1.911
4 2.162
5 3.061
6 3.469
7 4.034 1
8 5.282
9 6.266
10 9.664
' t" 0 / i 4
4.634
HEHORIZED
AREA UK
725
5761
3121
1879 V
1669
681
83771
599
443
1507
LHSUU TUBES
TOTAL
199556
IDHO
FILE
NETHOD
COMC
0
8002
NAME
ui
99.1366 CSS
0.8134 STYRENE
100
CJ
VI
6
10
-------
Z.7B9
LHSUU BAG SAMPLES
2.495
CR5B1 CHROHATOPAC
CHANHEL NO 2
SAMPLE HO 0
REPORT HO 81
FILE
METHOD
9
8082
PKNO
TIME
AREA UK IDM0
CONC
NAME
2
3
2.495
2.585
2.789
31523
1849 V
2623 V
2
94.4586 METHANE
5.5414 ETHANE
TOTAL
S5996
180
-------
MM
i- • I J 7
1:8?8
•
5.28
6. £63
IUDC.O
4.0
CHRONATOGRAM 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
£
I. 3 •
4
5
6
7
8
9
10
CHROMATOPAC
HO 1
HO 8
HO 82
TIME
1.391
1.594
1.9
£.159
3.95
3.468
4.032 1
5.23
6.263
9.661
AREA
7G8
5684
3053
1S5S
1667
676
82233
585
435
£350
MK IDNO
FILE
METHOD
COMC
6
B002
NAME
98.7263 CS2
'1.2732 STYRENE
11
9.791
TOTAL
1708 V
200354
01
100
-------
83
£
3
- 586
ID HO
9
Q6BS
91388
-------
10:5197/05/14
9 6 5
4.637
6. £65
9.65
CHROHATOGRAM 1 MEMORIZED
CR5Q1 CHROMATQPflC
CHANNEL HO 1
SAMPLE NO 8
REP.ORT NO 84
PKNO
TIME
LASCO TUBES
TOTAL
AREA MK IDNO
FILE
METHOD
CQNC
0
0003
NAME
1
£
3
4
5
1.905
4.037
5.277
6. £65
9.65
72972
213930
1287
3Q9
358
287955
99.8329 CS2
0.1671 STYRENE
180
-72
-------
97/85/14
O t • r, f-t m * 4
Cv- CC. • 1
-------
LASCO T
X
1.912
4.83
6. £59
'). &JD.4
££rrt
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 8
REPORT NO 36
FILE
METHOD
0
8002
PKNO
TIME
AREA MK I DUO
COHC
HAME
3
4
5
6
1.912
4.03
6. £59
6.922
9.654
10. 14
TOTAL
37/05/14
3107
191710
255
176763
380417
327G82
1079333
£3:42520
4 17. SI 74
3 16.4282
1 35.3557
£ 30.3987
100
Cr- ^
C' C
MM A
STYRENE
CUMEME
LASCO BAG SAMPLES
2.787
2.492
CR501 CHROMATOPAC
CHANNEL MO 2
SAMPLE HO 8
REPORT NO 87
FILE
METHOD
9
00G£
PKNO
1
2
3
TIME
2.492
2.585
2.787
AREA MIC IDNO
82117
3595 V
819 V
1
2
COMC
NAME
95.8956 METHANE
4.1944 ETHANE
TOTAL
86531
1G6
-------
£3:51:8797/05-
LASCO TUBES
.oX
1.914
4.G32
tn
to
< ff ' '•'•'a'lf
i U f i " T
I
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMP-LE HO 9
REPORT HO 88
6
N)
FILE
METHOD
0
0002
PKMQ
TIME
AREA UK IDHO
COHC
NAME
1
2
3
4
5
97/05/1
CR501
CHANNEL
SAMPLE
REPORT
1.914
. 4.032
6.926
9.658
10.144
TOTAL
5
2902
182653
162612
352150
301611
1001929
00:02:31
| 2.785 1-1UW"
CHROMATOPAC
NO 2
NO Q
NO 89
4 18.2831
3 16.2771
1 35.2493
2 30.1905
CSS ' '
MM A
STYRENE
CUMEME
100
LASCO BAG SAMPLES
FILE
METHOD
9
DO B 2
2.491
PKNO
1
2
3
TIME
2.491
£.583
2.735
TOTAL
AREA f1K IDHO
COMC
NAME
88350
3532 V
808 V
85189
95.8142 METHANE
4.1858 ETHANE
106
.-i A
-------
30:11:l397/85/15
LASCO TUBES
4.833
5.£79
6.262
9.653
CHROI1ATOGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHAMNEL MO 1
SAMPLE MO 9
REPORT NO 90
FILE
METHOD
0092
PKNO
TIME
TOTAL
4812677
o
o
AREA MK IDHO
COHC
NAME
1
2
Z
4
5
6
7
8
9
IB
11
12
13
14
1.597
1.916
3.931
4.033
5.279
6.262
6.925
9.309
9.411
9.653
10.133
19.442
10.55
19.857
645
1191
19563
157438
686
257
591376
15608
54213 V
3934626 VE
3216 V
2218
314 V
829
1
2
3.9735 CS2
12.5473 UNA
33.411 STYREHE
8.0682 CUMEME
ro
6
2
6
ro
1QG
-------
CR591
CHANNEL
SftttPLE
REPORT
PKNO
1
e
3
p-
£.784
i_ • sJ w i—
CHROHATOPAC
HO
HO
HO
2
2
2
2
8
91
TIflE
.49
.582
.734
AREA UK
28649
6158 V
318 V
FILE
METHOD
I UNO CONC
1 82.
2 17.
9
0002
HAME
387 METHANE
69S9 ETHANE
TOTAL
J5126
188
-------
1:!?*
3.027
==—
5.267
6.26
4.831
III:
Itf
9.658
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHROI1ATOPAC
CHANNEL MO 1
SAMPLE HO 0
REPORT MO 92
PKHO'
1
£
TIME
1.596
1.914
AREA UK I DUO
783
1301
FILE
METHOD
COHC
0
9082
NAME
3
4
5
6
7
8
9
10
11
12
13
14
3.027
4,031
5.267
6.26
6.924
9.311
9.414
9.658
18.144
10.45
10.558
10.866
£0173
186745
681
£52
579782
1.5092
52981
3894949
3286
£115
348
768
V'
VE
V
V
2
4.0033 CS2
12.429 MMA
83.4973 STYREHE
13.8784 CUMENE
KJ
KJ
TOTAL
4759162
100
-------
2.4'
2.785
CR5B1 CHROI1ATOPAC
CHflMHEL MO £
SAMPLE HO 0
REPORT NO 93
PKNO
1
£
3
TIME
2.49
2.583
2.735
AREA UK I DUO
.23793 1
6187 V £
311 V
FILE
I1ETHOB
COHC
9
0082
NAME
82.3133 METHAhE
17.6867 ETHANE
TOTAL
35290
100
-------
CHROMATOGRAM 101
57/65/15
MEMORIZED
17:24:51
LASCO BAG SAMPLES
•
f*
2.495
CR5Q1 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO
REPORT NO
PKNO
1
2
0
143
TIME
2.495
£.582
2.737
AREA MIC IDHO
19998 1
1789 V 2
738 V
PILE
METHOD
CONC
9
8862
HAI1E
TOTA".
£1535
91.3987 METHANE
8.6013 ETHANE
t4 0 ~ ~-
-------
CHROMATOGRAM 101 MEMORIZED
37/95/19 12:27:40
LASCO BAG SAMPLES
STDl
1.497
CR581 CHROMATOPAC
CHAMMEL MO 2
SAMPLE MO 9 .
REPORT NO 193
PKNO
1
2
TIME
£.497
2.589
AREA MK IDM0
13777
2 £89 V
FILE
METHOD
COMC
9
QB92
NAME
85.7541 METHANE
14.2459 ETHAME
TOTAL
16Q66
18D
-------
CHROHATOGRAM 101 MEMORIZED
?7/05/19 12:18:53
L. • ^J 'J 7
LASCO BAG SAMPLES
2.497
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 8
REPORT NO 192
FILE
METHOD
9
8002
to
to
CJ
6
PKNO
1
£
TIME
2.497
£.589
AREA UK IDNQ
13897
£30£ V
COMC
NAME
£
85.7984 METHANE
14.2G96 ETHANE
TOTAL
16199
100
-------
CHRQHflTOGRAH 1Q
37/85/19
1 £: G1: 15
LftSCO BAG SAMPLES
£.495
CR581 CHROtlATOPAC
CHflMHEL MO £
SAMPLE HO 8
REPORT NO 191
FILE
METHOD
9
9BQS
'KMO
1
TIME
£.495
£.587
TOTAL
AREA MK IDM0
COMC
NAME
129S6
£158 V
1
£
35.7491 METHANE
14. £509 ETHANE
15145
139
-------
CHROHATOGRAH 181
17/05/19
MEMORIZED
11:51:44
•:« t
LASCO BAG SAMPLES
2.496
CR5G1 CHROMATOPAC
CHANNEL HO 2
SAMPLE NO 8
NO 198
REPORT
FILE
METHOD
9
8082
PKNO
1
*s
c
TIME
2.496
2.58? '
AREA
13813
2284
t1
V
TOTAL
1S89?
COHC
NAME
85.889 METHANE
14.191 ETHANE
188
-------
CHROHATOGRAH 101 MEMORIZED
57/95/19 11:48:34
LASCO BAG SAMPLES
r
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE HO 8
REPORT HO 189
2.493
FILE
METHOD
9
GQ82
ro
Ni
s
Ni
o
PKNO
1
2
TIME
2.493
£.586
TOTAL
AREA UK IDNO
COHC
NAME
68690
6201
91.7195 METHANE
8.2804 ETHANE
74891
18 Ei
-------
CHROMATOGRAM 101
37/65/19
MEMORIZLLi
11:£9:18
I
LASCO BAG SAMPLES
L. • >.' V Q
STB
2.494
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 9
REPORT MO 188
FILE
METHOD
9
0802
PKNO
1
£
TIME
£.494
£.586
AREA HK I UNO
71464
6426 V
1
c!
CQNC
NAME
91.75Q3 METHANE
8.2497 ETHANE
TOTAL
7789Q
100
-------
;HRGI1ATOGRAt1 1G1 MEMORIZED
37/95/19
11:13:31
LASCO BAG SAMPLES
572>Z
/AID
2.491
CR5G1 CHROMATOPAC
CHANNEL HO 2
SAMPLE NO 9
REPORT HO 18?
PKMO
1
o
TIME
2.491
2.584
AREA MK I UNO
FILE
METHOD
COHC
9
0002
NAME
636S5
6178 V
91.7474 METHANE
8.2526 ETHANE
TOTAL
4863
100
-------
;HROMATOGRAM 101
37/65/19
MEMORIZED
10:50:40
LASCO BAG SAMPLES
CR501 CHROMATOPAC
CHflMHEL NO £
SAMPLE NO 0
REPORT NO 186
ro
ro
OJ
6
ro
O
CO
FILE
METHOD
9
0002
PKHO
1
£
TIME
2.491
£.535
TOTAL
AREA MK IDHO
134917
57455
O 1' ~? O
i_ •-' f C
COHC
HAME
76.2947 METHANE
£3.7052 ETHANE
5fZ)J
100
-------
CHROHATOGRAtl 101
37/65/19
18:45:££
LASCO BAG SAI1PLES
CR501 CHROMATOPAC
CHAMMEL NO £
SAMPLE HO G
FILE
METHOD
9
0BO£
REPORT NO 185
PKHO TIME
1
£.49
£.532
TOTAL
AREA MK IDHO
189788
5897£ V
'g.4875£
COHC
HA HE
76.2929 METHANE
£3.797 ETHANE
180
-------
CHROHATOGRAH 101
57/95/19
MEMORIZED
1 d: 1E: 13
r
LftSCO BAG SAMPLES
I
l.SIt
CR5BI CHROHATQPAC
CHANNEL MO £
SAMPLE HO 8
REPORT NO 184
PKHO
1
E
TIME
1.489
AREA UK IDNO
197996
61355 V
FILE
METHOD
CONC
9
eeee
NAHE
76.343 METHANE
S3.657 ETHANE
TOTAL
259351
1GO
-------
CHROMATQGRAN 101 MEMORIZED
97/65/li9 18:00:89 LASCO BAG SAMPLES
WARMING NO PEAK
CHROI1ATOGRAM 101 MEMORIZED
37/95/19 18:04:19 LASCO BAG SAMPLES
v
CR501 CHROHATOPAC
CHANNEL HO £
SAMPLE HO 8
REPORT NO 183
LJ
I
00
FILE
METHOD
9
SB6S
PKNO
TIME
AREA MK IBMO
CONC
.NAME
£.433
£.53
188S55
53495
76.2938 METHANE
23.7S6E ETHANE
TOTAL
£46751
108
-------
CHRQMATOGRAM 1G1
07/95/19
[1EI10RIZED
89:53:03
LASCO BAG SAMPLES
CR591 CHROHATOPAC
CHANNEL HO £
SAMPLE MO 9
REPORT NO 182
FILE
METHOD
9
0002
PKNQ
1
£
TIME
£.488
£.579
AREA IIK IDHO
733
1838 V
CONC-
HA ME
41.5542 METHANE
58.4458 ETHANE
TOTAL
1776
100
-------
CHRQMATQGRAN 1Q1
67/85/19
HARMING HO PEAK
CHROMATOGRAM 191
MEMORIZED
09:48:07
MEMORIZED
99:43: 13
LASCO BAG SAMPLES
LASCO BAG SAMPLES
CR5G1 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO G
REPORT HO 131
PKNO
1
TIME
£.487
£.578
TOTAL
AREA UK I DM0
741 1
1093 V £
1834
FILE
METHOD
CONC
9
BBB2
HA ME
49.4145 METHANE
59.5S55 ETHANE
106
-------
CHRQMATQGRAM 1Q1 MEMORIZED
37/95/15 £3: 38: £3
f £.781 l"w"
CR5Q1 CHROMATOPflC
CHAMMEL NO £
SAMPLE MO 8
REPORT HO 179
PKNQ TIME AREA MK I DM0
1 2.489 94425 1
£ £.579 4115 V £
3 £.731 1054 V
TOTAL 99594
LASCO BAG SAMPLES
C
FILE 9
METHOD G00£
COMC MAME
95.8239 METHAME
4.1761 ETHAME
100
£.489
-------
;HROMATOGRAM 101
37/95/15
MEMORIZED
23:34:43
£.731
.ASCO BAG SAMPLES
2.489
CR5B1 CHROMATOPAC
CHflMHEL HO £
SAMPLE NO 8
REPORT HO 178
PKNO
1
£
TIME
£.489
£.58
£.731
AREA MK IDNO
FILE
METHOD
CQNC
y
QGB£
NAME
97652
4236
1087
95.3423 METHANE
4.1571 ETHANE
6
ro
O
OJ
•vj
6
102975
100
-------
2.489
CR581 CHROMATOPAC
CHANNEL HO 2
SAMPLE NO Q
REPORT NO 177
PKNO
TII1E
TOTAL
AREA UK I DUO
1
2
3
2.489
2.577
2.782
21186
1691
1527
244Q3
FILE
METHOD
CONC
Q
80G2
NAME
92.6091 METHAME
7.3909 ETHANE
108
-------
CHRQMftTQGRftll 181 MEMORIZED
57/85/15 £3: £6: 08
01
CHANNEL HO £
SAMPLE NO 9
REPORT HO 176
LASCO BAG, SAMPLES
c . f o 4
OPAC
FILE
METHOD
! 9
i eee£
2.489
&
KHO
1
c
3
TIME
2.489
£.577
£.784
AREA UK
22526
1797 V
1626 V
ID NO
1
£
COHC
92.
7.
6199
3891
TOTAL
NAME
25949
U39
-------
37/85/15
•;. n t < c • c c
CO* 1 J • J J
LftSCO BflG SAMPLES
<
£.781
2.483
CR501 CHROHflTOPAC
CHAMMEL MO S
SAMPLE NO O
REPORT HO 175
FILE
flETHOD
o
OJ.
C'J
PKNO TIME AREA MK IDHO
£.438 98149
£.579 41£8
£.781 976
COMC
NAME
S
95.5639 METHAHE
4.036 ETHANE
TOTAL
193253
100
-------
C3:84:3197/05/1 5
1.91 £
3.Q4
•
5. £64
4.GS8
r
9.645
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAMMEL NO 1
SAMPLE HO 8
REPORT MO 174
LASCO TUBES
PKMO
TIME
TOTAL
AREA MK IDM0
FILE
METHOD
COMC
0
800S
HAME
1
l-t
'-,
•j
4
5-
1.
•j •
4.
5.
9.
91£
84
828
264
645
576
553
194827
1720
19358
4
1
90.
9.
9 6 1 9
Q3S1
217034
100
-------
97/Q5/1I5
D cif-:Db5c;4 LflbUU BAG 'oHnPLLs
f— — £.775 u.^ui
CHRQMATQPAC
NO £ FILE 9
HO 9 METHOD BQ0£
f9J < £>
i*>X * ^A w
A 6
>i A\ o
i^ t.\
6
N>
SAMPLE HO
REPORT NO 173
PKMO
1
£
3
TIME
2.489
£.581
£.775
AREA UK I UNO
97436
41£5 V
972 V
CONC
NAME
95.9382 METHANE
4.6618 ETHANE
TOTAL
18£
180
-------
97/85/15
££:37:03
LftSCO BAG SAHPLLO
£.489
CR5B1
CHAMM
SAMPLE HO
REPORT HO
PKMO
CHROflATOPAC
HO £
HO 8
HO 171
TIME AREA
£.489 670
TOTAL 670
2£M5: 1997/05/15
1.915
•:• iti o •:•
•j.i U ij ^'
5. £69
i 0 te. 0
FILE 9.
METHOD : 900£
MK I DM0 COMC MAME
1 100 METHANE
100
LASCO TUBES
r
CHRQMATQGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAMMEL MO 1
SAMPLE MO 0
REPORT HO 172
PKNO
TIME
AREA MK IDNO
FILE
METHOD
COMC
O
0002
NAME
1
£
3
4
5
1.915
3.033
4.032
5. £69
9.652
614
564
195750
1738
19431
4
1
90.9698
9.0301
TOTAL
318097
100
-------
£2:£553997/05/15
1.916
3.Q33
5.269
4. 035
LASCO TUBES
•
CHROMATOGRAM 1 MEMORIZED
CR5Q1 CHROI1ATOPAC
CHANNEL NO 1
SAMPLE NO 0
REPORT NO 17Q
PKHO
TIME
TOTAL
AREA MK IDM0
FILE
METHOD
cone
8
00B2
NAME
1
£
3
4
5
1.916
3.033
4.035
5.269
9.645
575
671
196568
1986
125805
4
1
60.9753
39.0247
325604
100
ro
M
U)
ro
o
CJ
VI
e
-------
97/05/15
O D • 1 ~> • 1 Q
\- C • if • •!• J
p £.775
LflSCO BAG SAMPLES
2.49
CR501 CHROMATQPAC
CHANNEL MO £
SAMPLE NO 8
REPORT NO 169
PKMO
1
TIME
2.49
2.578
£.775
AREA MK
20989
1664 V
367 V
FILE
METHOD
COHC
NAME
92.6564 METHANE
7.3436 ETKAHE
TOTAL
£3020
100
-------
66:1597/95/15
LASCO TUBES
1.913
3.04
4.031
5. £58
CHROHATQGRAH
1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 168
PKMO
TII1E-
AREA KK IDHO
FILE
METHOD
CDMC
Q
0082
NAME
o
•vl
b
e
r1
i
1
£
O
O
4
5
1.913
3.04
4.031
5. £58
9.651
533
667
194588
1963
121917
4
1
61.4882
33.5193
TOTAL
319734
-------
97/65/15
•-i i i c r, » i ,1
C 1 • j 0 • 1 4
LASCO BAG SAMPLES
el
2.489
CR561 CHROHftTOPAC
CHAHHEL NO 2
SAMPLE HO Q
REPORT NO 167
PKHO
3
TIME
.489
.57?
.782
TOTAL
AREA UK IDNO
28891 1
158E V 2
346 V
FILE
METHOD
COHC
80Q£
HAHE
21929
92.6712 METHANE
7.3288 ETHANE
188
-------
CHROHAT
Jl: 46: 5 197/05/1 5
1.908
— ^— —
-• •< W-( 1 •-
» v . i •.
OGRAtt 1
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO O
REPORT HO 166
PKNQ TIME
1 1.903
£ 4.026
3 6.913
4 9.65
5 10.135
4.026
,-
•.'
MEMORIZED
AREA MK
£204
193795
170309
374306
323555
LHbUU IUBLS
FILE 0
METHOD 0002
IDNO COHC NAME
4 18. £488 CSS
3 16.G371 MMA
1 35. £466 STYRENE
2 30.4676 CUMEME
TOTAL
1Q64169
196
-------
CHROI1ATOGRAM 181 MEMORIZED
37/95/15 £1:35:40
£. 7 8 5
LASCO BAG SAMPLES
£.431
CR5Q1 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO 9
REPORT MO 165
FILE
METHOD
9
800£
o
CJ
PKHO
i
£'""
TIME
£.491
£.584
£.785
TOTAL
AREA UK IDHO
38748
3548
948
COMC
HAME
96.1555 METHANE
3.3445 ETHANE
10Q
In A
-------
37/65/15 £
^IIWIAAbb*/
1 . 'i -> . r o
1 • C. f • J O
WARMING MO PEAK
CHROHATQGRAM 101 MEMORIZED
37/05/15 £1:31:07
• — 1.264
r£.501
£.803
CR501 CHROMATOPAC
CHANNEL MO £
SAMPLE MO O
REPORT HO 164
PKNO TIME
1 1.264
£ £.£07
3 £.£99
4 £.501
5 £.803
AREA MK
673
93350
3727 V
9 9 £
££4
LASCO BAG SAMPLES
LASCO BAG SAMPLES
FILE ' 9
METHOD 000£
IDNO CONC MAME
i 100 METHANE
TOTAL
93966
100
lad
-------
;HRCit1ATOGRAi1 181
37/05/15
MEMORIZED
£l:£4:£5
"36
LASCO BAG -SAMPLES
£.49£
CR501 CHROMflTOPftC
CHANNEL NO £
SAMPLE HO 8
REPORT HO 163
PKHO
1
TIME AREA UK IDM0
£.49£ 18343
£.58 1496
£.736 1338
. TOTAL £1677
TILE
METHOD
COMC
Q
G90£
NAME
9£.46G1 METHANE
7.5399 ETHANE
108
1(0
-------
120:36:4697/95/15
1.908
3. 047
I^B^^^^MH
5.269
6.26
4.933
LASCO TUBES
CHRQNftTQGRftN
CR501 CHROMATOPAC
CHflHMEL HO 1
SAMPLE MO 0
REPORT HO 160
MEMORIZED
PKNO
TIME
AREA MK IDHO
FILE
METHOD
CONC
0
GOBS
HA HE
10
ro
LJ
-------
iu: Df. c^y//
• 1.914
=
6.262
I A W •
CHROttflTOGRAII 1
CR501 CHROMATOPAC
CHANHEL HO 1
SAMPLE HO Q
REPORT HO 161
PKHO TIME
1 ., 1.914
£ v', 4.036
3' I' b.£6£ "
4 6.9£4
5 9.654
6 18.138
US/ID LHSCO TUBLS
6^
4.036
i- - ---'
MEMORIZED
t
FILE 0
METHOD G002
AREA flK I DM0 COMC HA ME
2473 ."'• '- ..
1^944£ , 4 18.0444 CS£
, 261
177854 3 16.0913 MHA
391349 1 35.4Q71 STYRENE
336637 Z 30.4572 CUHEME
TOTAL
1108816
100
-------
17:6397/05/15
1.918
3.85
CT •"> "7 '
D. cY i
4.034
CHROHATOGRAH 1 MEHORIZED
CR501 CHROHATOPAC
CHAHMEL HO 1
SAMPLE HO 0
REPORT HO 159
LASCO TUBES
PKHO
TII1E
AREA MK IDHO
FILE
METHOD
CQNC
O
000E
HA HE
1
c
•-I
•^
4
1.918
3.05
4.034"
5.272
TOTAL
863
1 "i £
• :• o D
192912
2011
196122
4 100
100
-------
37/65/15 19:48:41
LASCO BAG SAMPLES
\-
— -£.78^"
CR5B1 CHROMATOPAC
CHANNEL
NO £
SAMPLE NO 9
FILE : 9
METHOD i 00B2
REPORT NO 157
PKNO
1
£
3
CHROI1AT
CR5B1
CHANNEL
SAMPLE
REPORT
PKNO
1
£
3
4
5
6
7
TIME
£.495
£.583
£.788
TOTAL
AREA MK
17736
1494 V
7 1 1 V
19941
19:57: 1197/95/15
1.998
3.033
5. £71
6.262
OGRAM 1
CHROMATOPAC
NO 1
NO 8
NO 158
TIME
1.908
3.033
4.033
5. £71
6.262
9.659
10. 146
4.033
MEMORIZED
AREA MK
412
1078
194870
1981
266
162860
378
IDNO COMC NAME
1 92.2287 METHANE
£ 7.7713 ETHANE
180
LASCO TUBES
FILE 0
METHOD 00G2
IDNO COMC NAME
4- 54.4166 CS2
1 '45.4778 STYRENE
2 8.1057 CUMEME
2.495
I
IS)
O
6
to
TOTAL
361846
100
-------
19:37:1597/95/15
1.92
3.945
5.273
4.G36
1 U.loo
CHROMATOGRAM 1 MEMORIZED
LASCO TUBES
CR501 CHRQHATOPAC
CHAHHEL HO 1
SAMPLE HO 0
REPORT HO 156
FILE
METHOD
0
oeee
PKNO
TIME
AREA UK IDHO
COHC
HA HE
1
c!
X
4
5
6
1.
^i
O •
4.
5.
9.
IB.
92
045
036
£73
657
133
414
1087
193737
1964
153837
354
• 4
1
c
54.
45.
0.
3942
0055
1 D 0 3
CS2
STYRENE
CUME ME
TOTAL
356393
10G
ttf
-------
97/S5/15 19: £8:
CR5G1 CHROMATOPAC
CHANNEL NO £
SAMPLE HO Q
REPORT NO 155
LASCOJ8AG SAMPLES
PKNO
1
TIME
2.496
TOTAL
AREA MK IDHO
679 1
679
FILE
METHOD
CONC:
190
180
9
009S
NAME
METHANE
I
W
VI
6
ro
-------
57/85/15 19:08:40
LASCO EAG SAMPLES
I
.
£.49
CR501 CHROMATOPAC
CHANNEL NO 2
SAMPLE NO 8 *•
REPORT NO 153
V
FILE
METHOD
^0002
>KNO
1
*-t
TIME
AREA UK IDHO
2.49
2.5!
-' 581
4833
186
TOTAL 501'
19: 17:1697/85/15
1.9-18
3.052
5. £75
4.839
CHROI1ATOGRAM 1 MEMORIZED
CR5D1 CHROMATOPAC
CHAMMEL NO 1
SAMPLE NO 3
REPORT NO 154
1
2
CONC
NAME
96.2915 METHAHE
3.7065 ETHANE
100
LASCO TUBES
FILE
METHOD
0
8002
PKNO
TIME
AREA MK IDHO
CONC
NAME
1
2
3
4
1.918
3.052
4.639
5.275
1222
343
195222
2069
TOTAL
198857
100
lOD
CSS
-------
97/85/15
18:48:48
LASCO BAG SAMPLES
r"" £. 787 "~ ' Ou°
CR581 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 8
REPORT HO 151
PKNO
1
£
3
TI
ME
2.493
£.585
£.787
TOTAL
I8i57:i797/
1.
Cl •
919
G51
AREA MK
106829
4273 V
1038 V
112139
05/15
FILE 9
METHOD 8G8£
IDNO COHC NAME
!• 96.1541 METHANE
£ 3.8459 ETHANE
100
LASCO TUBES
•• V
2.493
5. £74
CHRGMATGGRAM
1 MEMORIZED
CR5G1 CHROMATOPAC
CHANNEL HO 1
FILE
o
iO
•o
SAMPLE
REPORT
PKNO
' 1
£
3
4
MO 0
MO 152
TIME
1.919
3.051
4.837
5.274-
AREA MK
1228
343
196598
2087
METHOD 1
IDNO COHC
4 186
6682
NAME
CS2
K)
K)
OJ
Nl
6
K)
TOTAL
200256
100
-------
LASCO TUBES
1.919
3.044
•—
5. £74
6.93
4.037
fO
fO
o
CJ
VI
6
Is)
19.14
CHROI1ATOGRAM 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKMO
4
£
3
4
5
6
7
CHROtlATOPAC
NO 1
HO 0
HO 150
TIME
1.919
3.044
4.037
5.274
6.93
9.657
10. 14
AREA MK
749
1834
193385
1618
583
78£920
11£3
I DUO
4
3
1
tl
FILE
METHOD
COHC
Q
000£
NAME
19.7744 CS£
3
1
tl
Q.
SO.
0.
8535
8567
1154
MMA
STYREHE
CUMEME
TOTAL
982349
10Q
-------
•3 : i f • i 0 y / f i
1.914
3.037
— — —
5.269
6.261
6.929
10.145-^'
CHROMATOGRAM 1
CR581 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO O
REPORT HO 148
PKMO TIME
1 T.914
2;, 3.037
3'' 4.03
4« 5.269
5 6.261
6 . 6.929
7 9.659
8 10.145
j D / 1 ;•
4.83
™
MEMORIZED
AREA MK
733
1789
139241 /
1714- >"
252
499
742801
1072
LHbtU MJULo
FILE G
METHOD 0002
IDHO COMC NAME
4 20.2697 C32
3 G.B534 HHA
1 79.562 STYREHE
2 . O. 1148 CUMEME
TOTAL
938091
100
-------
57/85/15 13:03:48
£.736
LASCO BAG SAMPLES
• -j 'j -J
2.492
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 0
REPORT HO 147
PKNO
TIME
2.492
£.585
9 ~7 O f
u . i uO
TOTAL
AREA MK IDNQ
TILE
METHOD
COHC
9
8802
NAME
K)
K)
CO
6
184513
4190
1824
189731
96.1459 METHANE
3.8541 ETHANE
100.
-------
|17: 52: £297/65/15
LASCO TUBES-
4.839
r 1.9H
3. 05
5.272
6.265
9.656
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAMMEL NO 1
SAMPLE HO 0
REPORT HO 146
PKNO
TIME
TOTAL
1
£
3
4
5
6
1.
3.
4.
5.
6.
9.
914
05
039
£72
£65
656
6735
945
218877
8841
316
3437
£39151
MK I DM.0
FILE
METHOD
COMC
0
0002
NAME
98.4542 CS2
1.5458 BTYREHE
100
-------
57/05/15
17:44:39
LASCO
o
to
o
2.492
CR5Q1 CHROI1ATQPAC
CHAMMEL NO £
SAMPLE MO 0
REPORT HO 145
PKHO
c
3
TIME
£.492
£.53
£.736
TOTAL
AREA MK IDNO
13235 1
1518 V £
699 V
FILE
METHOD
COHC
0962
NAME
92.3163 METHANE
7.6836 ETHANE
£9451
109
-------
il7:33:04':V/05/15
r i • 31 a
3. 846
"" 5.271
6. £63
9.655
CHROMATOGRAM
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT HO 144
4.636
MEMORIZED
PKMO
TIME
AREA HK
1
e -.
••>
•_'
4
C
•j
1.
•-' •
4.
5.
6.
91£
046
836
£71
263
6338
3S9
212453
8374
297
LASCO TUBES
BHO
FILE
METHOD
CDNC
8
0002
NAME
S8.4714 CS2
9.655
TOTAL
3298.
231658
1.5286 STYRENE
1GB
-------
to
CJ
6
IO '
6
ro
WARNING HO PEAK
UARNIHG HO PEAK
CHROMATOGRAH 1
WARM IMG MO PEAK
CHROMATOGRAM 131
MEMORIZED
MEMORIZED
£.486
CR581 CHROMATOPAC
CHANNEL HO £
SAMPLE NO 8
REPORT HO 3
PKNO
f
£
TItlE
2.486
£.577
AREA MK IDNO
3971
3961
FILE
METHOD
CONC
9
000£
NAME
2
£
74.558 ETHANE
£5.44£ ETHANE
TOTAL
1S033
lOO
-------
CHROHATOGRAtl 1 MEMORIZED
WARMING MO PEAK
WARNING NO PEAK
K)
K)
U
6
to
o
CJ
•N
6
N)
CHROMATQGRAH 1 MEMORIZED
WARNING HO PEAK
CHROMATOGRAM 101 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 3
SAMPLE HO Q
REPORT HO 4
PKNO
1
2
TIME
8.345
£.436
TOTAL
AREA UK IDM0
3684
8942 V 1
11545
FILE
METHOD
CONC
180
180
9
0002
NAME
METHANE
-------
CHROMATQGRAM 1G1 MEMORIZED
£.481
CR501 CHROMATOPAC
CHANNEL HO £
SAMPLE NO 0
REPORT NO 5
:'KHO
TIME
2.481
AREA MK !DHO
3664 2
£966 V £
FILE
METHOD
COHC
9
000&
HA ME
74.4947 ETHANE
£5.505£ ETHANE
TOTAL
11630
106
-------
^7/05/14 88:19:01
LASCO BAG SAMPLES
CR5B1 CHROttATOPAC
CHANNEL NO £
SAMPLE HO 8
REPORT HO 6
FILE
METHOD
9
Q88£
10
CO
6
3
CO
PKHO
HUE
AREA UK IDHD
CONC
HA HE
£.482
£.575
TOTAL
19333
£
£
£3.3834 ETHANE
76.6916 ETHA-HE
3E968
188
-------
':' 0 : £ -3 : u f
r
LASCO BAG SAMPLES
©
lltff
CR5G1 CHROHATOPAC
CHANNEL HO £
SAMPLE HO Q
REPORT MO 7
PKNQ
1
£
TIME
£.432
£.575
AREA UK IDNO
18620
61370 V
FILE
METHOD
CONC
609 £
NAME
23.2777 METHANE
76.7££3 ETHANE
TOTAL
9989
100
-------
CHROMAT
CR501
CHANNEL
SAMPLE
REPORT
OGRAM 191 MEMORIZED
37/85/14 08:41:55 ' LASCO BAG SAMPLES
CHROMATOPAC
HO 2 FILE 9
HO 0 METHOD 0002
HO 8
FKNO TIME AREA MK IDNG CQNC NAME
1 2.482 32195 1 85.0304 METHANE
2 2.574 5668 V 2 14.9696 ETHANE
:••*
TOTAL
37862
100
-------
97/95/14 99:81:38
CHROMATOGRAI1 1 MEMORIZED
WARNING NO PEAK
03:02:23 97/05/14
LASCO BAG SAMPLES
LASCO
CHROMATOGRAM 1 MEMORIZED
WARNING NO PEAK
97/85/14 99:02:53
FARMING HO PEAK
97/05/14
CHROMATOGRAM 1 MEMORIZED
WARNING NO PEAK
CHROMATOGRAM 101 MEMORIZED
07/65/14 09:03:££
WARNING NO PEAK
LASCO BAG SAMPLES
LASCO
LASCO BAG SAMPLES
RT CHECK STYRENE
119:20:2797/05/14
LASCO TUBE!
ilf
-------
CHROMATC
I
iGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHAMMEL HO 1 FILE G
SAMPLE NO 0 METHOD 088£
REPORT HO 19
PKHO
1
£
CR501
CHANNEL
SAHPLE
REPORT
PKMO
1
TIME AREA MK I DUO COHC NAME
1.893 59471
4.Q16 188389
TOTAL £38860 0
*7/05/14 09: £5= 45 LASCO BAG SAMPLES
1 £.56? ;- =
CHROMATOPAC
HO £ FILE 9
HO 0 METHOD 800£
HO 11
TIME AREA MK I DUO COHC HAME
£.567 129 £ 100 ETHANE
TOTAL 128 180
4.016
-------
39:43:2497/65/14
LASCO TUBES
4.016
9.633
-------
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO. O
REPORT NO 12
PKNO
TIME
AREA NK IDHO
FILE
METHOD
CONC
000E
NAME
fOl
ol
col
to
1
£
3
4
5
6
7
8
9
10
11
12
13
14
1.896
4.016
6.233
8.712
9.068
9. £93
9.633
10.13
10.438
10.733
10.845
10.941
11.021
13.375
47218
179905
233
651
£28 V
1353
4589262 VE
1272 V
665 V
866
1856 V
494 V
339 V
690
15
16
17
13.758
14.292
14.577 .
£613
4169
£2863
TOTAL
4854674
-------
16:18:£997/95/1 4
LASCO TUBES
i .396
4.016
6. £33
8. 71
Y_Ji!¥
\ lift-A**
v. ijferf
•3,633
o • < -j o
K)
IO
CR581 CHROHATOPAC
CHftMMEL MO 1
SAHPLE MO 0
REPORT MO 13
PKHO
TIME
AREA MK IDHO
FILE
'METHOD
CONC
0
000£
NAME
1
2
3
4
5
1.896
4.016
6.233
8.712
9,068
47213
179905
233
651
228
V
-------
0:13:5697/95/1'
LASCO TUBES
i.SOC
3.038
4.Q23
CHROMATOGRAM 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT'
PKNO
1
£
3
4
5
6
7
y
9
10
11
12
13
14
15
16
17
18
19
£0
£1
£2
£3
£4
- £5
26
CHROMATOPftC
NO 1
HO JJ.
HO V14r:;
TIME
1.396
3.038
4.023
6.242
7.958 '
8.533
3.967
9. £76
9.531
9.642
9.753
19.13
10.531
10.847
11. 125
11.413
11.667
12.B65.
1£.335
12.517
12.333
13.164
13.513
13.744
14.15
14.432
TOTAL
AREA
24422
302
137896
£7£
129
£593
6069
7983
6791
3829
6177
1275429
12025
13349
3446
11900
14047
16277
16148
9978
11331
.10054
7763
8950
5279
2383
4669713
MK
\!
•t
V
V
V
VE
V
V
V
V
V
V
V
V
V
V
V
V
V
V
IDNO
FILE
METHOD
COhC
O
9QQ£
NAME
1
1
1
2
0.1576 STYRENE
0.0889 STYRENE
.0.1434 STYRENE
99.2323 CUMEME
0.3778 MMA
ND
tO
N9
100
-------
1697/05/14
1.896
LASCQ TUBES
4. 023
6. £51
16.125
CR501 CHRONATOPAC
CHANNEL MO 1
SAMPLE HO 0
REPORT
PKNO
1
£
3
4
. 5
6
7
8
9
18
11
12
13
14
NO 15
TIME
1,896
4.. 0£3
6.251
3.908
9.281
9.529
9.633
9.753
18. 125
10.422
10.531
10.S47
11.1
11.333
TOTAL
AREA UK
24174
186477
27£
£731
4099 V
3537 V
2072 V
2727 V
4264503 E
1082 V
1258 V
1687
396
792
4505029
I DM0
1
1
1
^\
c
FILE
METHOD
CQNC
NAME
8.6827 STYRENE
0.0485 STYRENE
0.0638 STYRENE
99.7343 CUME11E
100
-------
LASCO TUBES
4.025
7.63
10.725
CHROMATOGRAtl 1
CR581 CHROHATOPAC
CHANNEL MO 1
SAMPLE MO 0
REPORT HO 16
I1EI10RIZED
PKNO
4
5
8
9
10
11
TII1E
AREA HK IDHO
1.898
4. 025
6.925
7.68
3.896
9.221
9.515
9.646
9. 752
10.128
10.725
77543
193654
4248512
1075
5872
15397
13223
2294
7908
3518
633
FILE
•METHOD
CDNC
0
0002
NAME
o
CO i
Nl '
6
4.3499 CS2
95.0551 MMA
9.2964 STYRENE
0.0514 STYREHE
8.1773 STYRENE
8.0789 CUMEHE
TOTAL
4561678
100
-------
BLANK CS2
18:58:4197/95/14
i. 90C
«•
5. £58
6.924
4.U£9
CHROMATOGRAM 1 flEHORIZED
CR5Q1 CHROflATOPAC
CHAMMEL HO 1
SAMPLE NO 9
REPORT NO 17
PKMO
TIME
TOTAL
AREA
1
z
3
4
5
6
7
1.9Q2
4.0£9
5.258
6.924
9.335
9.657
9.958
73866
£00698
1153
466
2521
£258
1023
281976
LASCO TUBES
I UNO
FILE
METHOD
CQNC
9
0002
NAME
98.6651 CS£
0.2289 UMA
1.196 STYRENE
100
-------
ill: 19:3097/05/14
|- 1.911
4.036
LflSCO TUBES
b.265
CHROMATOGRAM 1 MEMORIZED
CR5G1 CHROMATOPAC
CHAMMEL HO 1
SAMPLE NO . 0
REPORT HO 18
PKHO
TIME
TOTAL
AREA flK IDHO
FILE
METHOD
cone
0
0002
450689
NAME
1
£
3
4
5
6
•j
f
8
9
1.
4.
6.
6.
9.
q
.• •
9t
10.
10.
911
036
£65
928
45
656
767
139
46
4199
£04551 4
235
45804 ';
1985
94290 V 1
2226 V
93703 V £
3646 V
46.6641 CS2
10.4492 MMA
21.5104 STYREHE
21.3763 CUMEME
Nil
100
-------
1:39:4897/85/14
1.91
4.832
6. £61
CHROHATOGRAtl 1 MEMORIZED
CR561 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 19
PKMO
TIME
LASCO TUBES
AREA UK IDMO
FILE
METHOD
COHC
OQQ£
HA HE
1
c
3
4
5
6
7
8
9
10
1.
4.
6.
6.
3.
9.
9.
10.
10.
10.
91
93 £
£61
917
753
177
653
135
£83
624
3541
133b£l
£43
38945
4593
£600 V
80317
78197
1581 V
£636
4
«-!
-j
1
'•S
C
48.
10.
£1.
£0.
4
£
0
5
r.
'_'
1
7
1
44
96
6£
98
CS2
I1I1A
STYRENE
CUMEME
TOTAL
3964
t o
100
-------
.OiJ STD LIQ/ RUM 1 OPEN 9 BAG
2:89:8997/65/14
r 1.913
4.034
6. £64
q 3
CHRQMATOGRAH 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT NO £Q
PKHO
••'A
£.
o
4
5
6
TIME
1.913
4.034
6. £64
6.9E7
9.3
9.656
10.139
TOTAL
433367
• ASCO TUBES
AREA MK IDM0
3996
198832 4
£79
44110 3
£335
9444£ 1
38874 V 2
FILE
METHOD
CQNC
0
8882
NAME
46.646 CS2
18.3482 MMA
££.156 STYRENE
£8.8498 CUMEME
188
I
ro
O
i
II
L
-------
37/05/14 12:11:36
2.785
LASCO BAG SAMPLES
'.49
CR5S1 CHROMATOPAC
CHANNEL NO £
SAMPLE HO 8
REPORT HO £1
PKHQ
TIME
AREA MK IDHO
FILE
METHOD;
cone
9
0802
1
£
3
£.49
2.583
2.785
TOTAL
188487
448S
1868
114629
V
V
I
2
96.8335
3.9675
iee
-------
- 1.913
LASCO TUBES
4.037
6. £66
10.537
CHROMATOGRAtl 1 MEMORIZED
CR5G1 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO G
REPORT "NO £2
CO
CO
PKNQ
TIME
TOTAL
AREA UK IDHO
FILE
METHOD
CQNC
8
8002
HAI1E
10
10
OJ
6
6
SJ
1
*•,
u
3
4
5
6
7
1.
4.
6.
6.
9.
10.
19.
913
937
£66
928
653
141
537
4543
2B44E8 '
£93
c'019£7
435506
382827 V
5471 V
4,
v".
o
O
1
2
16.
16.
35.
31.
7Q31
4988
5S38
2142
C32
HHA
STYREHE
CUMEI1E
1234195
100
-------
97/05/14
12:32:39
£.736
LASCO BflG SAMPLES
2.491
CR5Q1 CHROI1ATOPAC
CHANNEL HO £
SAMPLE HO O
REPORT HO £3
PKMO
TIME
AREA MK IDHO
FILE
METHOD
CONC
9
0GB2
NAME
1
£
3
2.491
£.584
2.786
TOTAL
185427
4375
1836
110838
V
V
96.8154 METHANE
3.9846 ETHANE
100
-------
12:41:3897/65/14
h 1.915
4.033
6.263
LASCO TUBES
CHROMATOGRAM 1 MEMORIZED
CR561
CHAMHEL
SAMPLE
REPORT
PKHO
1
£
3
4
5
6
7
8
CHROMATOPAC
NO 1
HO Q
HO £4
TIME
1.915
4.Q33
6.263
6.925
9.457
9.657
9.844
18. 143
AREA MK
4278
198658
277
192288
3058
406416 V
5644 V
350253
ID HO
4
'•i
J
1
2
FILE
METHOD
COHC
8
0002
NAME
17.3117 CS2
TOTAL
1165791
16.7496 MMA
35.4164 STYRENE
30.5222 CUMEME
1G0
\a(o
-------
ii::53:09
r
CR591 CHROflATOPAC
CHANNEL HO £
SAMPLE NO 8
REPORT NO 25
BAG SAMPLES
PKMO
1
TIME
2.491
TOTAL
AREA
195868
195068
FILE
METHOD
CONC
188
188
6
K)
2,
880£
NAME
METHANE
-------
h 1.914
3:82:1297/65/14
LASUU
4.04
6. £72
CHROI1ATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL MO 1
SAMPLE HO ' 8
REPORT
PKNQ
1
•.£: •
.' $:'•
4
5
6
7
8
9
10
11
12
HO 26
TIME
1.914
4.84
6.272
6.934
9.167
9.317
9.408
9.513
9.664
18.148
18.366
18.782
TOTAL
AREA !1K
4457
280713
234
195825
1788
736 V
643 V
749 V
415814
357324
2288 V
3467
1183921
IDNO
4
*-,
O
1
2
FILE
METHOD
COMC
8
8802
NAME
17.1597 CS2
16.7418 UNA
35.5495 STYREHE
30.549 CUMEI1E
188
-------
CJ
CR5G1
'CHANNEL
SAMPLE
REPORT
PKMO
1
37/8
r
5/14 13:13:48
CHROflATOPAC
HO £
HO 8
HO £7
T
£.
I ME AREA UK
493 132122
TOTAL 1921££
LASCO BAG SAMPLES
FILE 9
METHOD GQG£
IDNO CONC NAME
1 180 METHANE
190
to
K)
2.493 §
S
SI
6
-------
3:£2:£897/05/14
LASCD TUBES
1.918
4.Q42
I
6. £73
i \i\rn
CHROHATOGRAH 1 MEMORIZED
CR5G1 CHROMATOPAC
CHAMMEL NO 1
SAMPLE MO B
REPORT. HO £8
FILE
METHOD
8
8082
PKHO
T1I1E
AREA MK I UNO
CQNC
HA HE
1
£
3
4
5
6
7
3
9
1.918
4.84£
6.273
6.933
9.66
10.143
18.387
18.558
10.865
1851
2Q888E
305
449469
848540
785786
3412
450
2841
1
£
9. 1467 CS£
19.£877 MMA
37.1567 STYREHE
34.4088 CUI1EME
TOTAL
2292537
100
-------
'57/95/14
13:33:58
LASCO EAG SAMPLES
2.495
CR581 CHROI1ATOPAC
CHfiMNEL HO £
SAMPLE HO 8
FILE
METHOD
9
0982
REPORT HO 29
PKNO . TIME
1 £.495
£ £.585
3 2.789
TOTAL
CD
AREA tUC IDHO
CONC
HAI1E
32471
1886 V
923 V
35280
94.5104 METHANE
5.4896 ETHAHE
100
I/I
-------
3:4318397/85/14
LASCO TUBES
4
1.921
4,841
6. £71
CHROttATOGRftfl 1 HEHORIZED
CR581 CHROflATOPAC
CHANNEL NO 1
SAHPLE NO 8
REPORT NO 38
PKNO
1
£'
"3? •
4" .
5
6
TIME
1.9S1
4.041
6. £71
6.93£
9.661
10.145
AREA
1837
£98233
312
441514
353268
798985
TOTAL
£391541
FILE
METHOD
CONG
8
8B82
NAME
'3.856 CSS
19.2187 MHA
37.3255 STYRENE
34.3997 CUHEME
108
-------
37/65/14
13:54:29
LASCO BAG SftMPLES
OX
2.496
CR5Q1 CHROHATOPAC
CHANNEL MO £
SAMPLE MO Q
REPORT HO
il
PKMO
1
2
3
TIME
2.496
2.586
2.737
TOTAL
AREA HK IDHO
367Q5 I
£068 V £
2197 V
FILE
METHOD
CONC
9
0002
HftHE
94.6656 METHAME
5.3344 ETHANE
40971
180
-------
•14:11:4397/95/14
4.041
' •• ft r
* • .•' U O
5.275
6.£73
9.674
CHROMATOGRAM 1 MEMORIZED
CR561 CHROI1ATDPAC
CHANNEL HO 1
SAMPLE NO 0
REPORT HO 32
LASCO TUBES
PKNO
TIME
TOTAL
AREA MK IDHO
FILE
METHOD
CQNC
e
236549
NAME
1
•-.
c
•-.
4
5
1.906
4.041
5.275
6. £73
9.674
73862
203548
1250
£54
2594
•4
1
98
1
.7415
.2585
CJ
6
8
w
199
-------
i f f y D / 1
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
£
3
<\
=—
1 <» : d 3 : U b
£.7^9-'OJ
CHROMATOPAC
MO £
MO 0
NO 33
TIME AREA RK
£.495 £96£9
£.585 1731 V
£.789 354 V
LHbUU b'Hb bHnKLLb
FILE 9
METHOD 060£
IDMO COMC NAME
1 94.479 METHANE
£ 5.5£1 ETHANE
2.495
TOTAL
3££14 •
190
-------
OPEN 9 RUN £ BAG; BLANK LIQ
14:32:1897/05/14
LASCO TUBES
4.641
5.£82
6. £72
9.798
10.858
CHROHATOGRAH 1
CR5B1. CHROttATOPAC
CHANNEL NO 1
SAMPLE.. NO 8
REPORT NO 34
tlEttORIZED
FILE
METHOD
8
9002
>KMQ
TIME
TOTAL
AREA UK IDNO
1
£
3
4
5
6
1.969
4.841
5.282
e-.£72
9.793
18.858
79635
£83413
1245
£88
3398
£417
£90396
CONC
100
NAME
;s£
108
-------
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
2
3
37/85/14 14:43:4
1 £.79
CHROMATOPAC
HO 2
NO 8
NO 35
TIME AREA
2.496 117443
£.588 4766
2.79 1897
TOTAL 123306
4 LASCO BAG SAMPLES
u • O O O
PILE 9
METHOD 8002
MK IDNO COHC NAME
1 96.1081 METHANE
V £ 3.8999 ETHANE
V
180
2.496
-------
14:52:5497/95/14
4.94
5.281
6.£71
1
CHRGMATOGRAM 1 MEMORIZED
CR5Q1 CHROtlATOPAC
CHANHEL MO 1
SAMPLE NO G
REPORT MO 36
LASCO TUBES
PKNO
TIME
TOTAL
AREA UK IDHO
1
£
3
4
1.911
4.84
5. £31
fa. £71
77445
£0£5£0
1235
£85
£81484
FILE
METHOD
COMC
100
198
8
oees
NAME
CS2
I/O
-------
?7/85/14 15:82:18
LASCO -BAG SAMPLES
if*
2.49?
CR5B1 CHROI1ATOPAC
CHANNEL NO 2
SAMPLE HO 8
REPORT NO
37
PKHO
TIME
TOTAL
AREA UK IDHO
1 '
£
3
£.497
2.589
£.791 '
119759
4858
1119
1257£7
FILE 9
METHOD 81
cone
NAME
96. 1815 METHANE
3.8985 ETHANE
108
I
I
6
-------
15:89:3897/85/14
LASCO TUBES
1.918
4.B35
6. £67
CHROI1ATOGRAM 1 MEMORIZED
CR591 CHROMATOPAC
CHANNEL HO 1
SAMPLE. HO Q
REPORT HO 38
PKNO
TIME
TOTAL
AREA MK I DUO
FILE
METHOD
COHC
B
300£
HAtlE
1
£
3
4
5
6
7
8
1 . 9 1 S
4.035
6. £67
6.929
9.317
9.663
18.15
10.548
836
189702
£72
940651
£86
1946652
£418484
1999
549888£
3.45E CS£
17. 1168 MMA,
35.4-EE7 STYREHE
44.Q085 CUHEME
180
-------
27/85/14 15:21:61
LASCO BAG SAMPLES
2.496
CR5G1 CHROMftTOPftC
CHANNEL HO £
SAMPLE NO 8
REPORT HO 39.
PKHO
2
3
TIME
2.496
2.586
£.789
TOTAL
AREA t1K IBNO
34381
1937 V
406
36723
FILE
METHOD
CONC
£
NAME
94.6672 METHANE
5.3328 ETHANE
o
106
-------
07/65/15 13:48:24
£.787
LASCO BAG SAMPLES
2.493
CR561 CHROHATOPAC
CHANNEL HO 2
3AHPLE MO 0
REPORT HO 127
FILE
METHOD
9
088E
PKHO-
1
TIME
2.493
2.585
2.7S7
AREA m
99Q55
4296 V
921 V
IDNO
1
COHC
NAME
95.8485 METHANE
4.1515 ETHANE
TOTAL
184267
1QQ
-------
L. , i ^ o u lUIiLD
- 1.9B7
4,0;
5. £58
CHRQMATOGRAH 1 MEMORIZED
CR5Q1 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT HO 128
F'KNO
1
£
TIME
1.9Q7
4.03
5.253
AREA M!< I HMO
4888
191645
3
FILE
METHOD
COMC
100
131
0
9002
NAME
CSS
TOTAL
198266
ISO
-------
97/95/1.5
14:00:27
LASCO BAG SAMPLES
£.736
2,491
CR501 CHROMATOPAC
CHANNEL HO £
SAMPLE HO O
REPORT MO 129
PKMO
TIME
AREA IIK IDNO
FILE
METHOD
COhC
9
8092
NAME
1
£
3
2.491
2.584
2.736
99985
4332
937
1
V £
V
95.3469
4. 1531
METHANE
ETHANE
TOTAL
105254
100
-------
1.921
3.842
===^^—
5.267
6.931
— 9.65
CHROMATOGRAM . 1
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 130
PKNO TIME
1 1.921
£ 3.042
3 4.036
4 5.267
5 6.931
6 9.65
4.036
MEMORIZED
AREA f1K
323
451
188643
. 743
1317
10949
FILE
METHOD
IDHO CONC
4 93.8983
3 =;•"'"• 8.6557
lv< t..:\r.. .5.4455
0
o
i
NAME
TOTAL
202418
100
-------
14:29:1997/05/15
LASCO TUBES
1.923
3.842
5.£78
6.265
6.932
4.838
r
9.659
CHROI1ATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL NO 1
SAMPLE MO 9
REPORT MO 132
PKMO
1
2
TIME
1.923
3.042
4.Q38
5.£78
AREA MK I UNO
407
1 c> 5 7
217486 4
924
FILE
METHOD
COMC
O
0002
NAME
93.4623 CS2
o
fO
6
7
6.265
6.932
9.659
TOTAL
315
1672
13536
234816
0.7187 MMA
5.3191 3TYREME
100
to
fO
to
6
ro
O
\L(f.
-------
CHR0MATOGRAM 1 MEMORIZED
WARNING HO PEAK
14:41:1997/05/15 LASCO TUBES
CHRQI1ATOGRAI1 1 MEMORIZED
WARNING NO PEAK
|14!49: 1797/95/15
1. 91 6
5.273
6. £61
9.992
4.633
CHROI1ATOGRAI1 1 MEMORIZED
01 CHROMATOPAC
CHANNEL HO 1
SAHPLE HO 0
REPORT MO 134
PKNO
TIME
1
E
3
4
5
1.916
4.033
5.273
6. £61
9.992
98G
£94983
963
£65
33664
TOTAL
£40800
LASCO TUBES
AREA MK IDNO
FILE
METHOD
COMC
180
8
0082
NAME
CS2
-------
37/95/15 15:06:39
WARNING HO PEAK
15509:9597/05/15
1.916
5. £75
4.034
> 9.993
CHROMATOGRAM 1 MEMORIZED
CR5G1 CHROtlATOPAC
CHANNEL HO 1
SAMPLE HO B
REPORT HO 135
LASCO BAG SAMPLES
o
to
LASCO TUBES
K>
ro
N»
PKHO
TIME
AREA MK I DUO
1
£
3
4
1.916
4.034
5.275
9.993
S55
188834
314
17DO^7
* O C'yV t
FILE
METHOD
CONC
100
NAME
cse
TOTAL
369359
100
-------
5:28:3797/85/15
\- 1.986
3.Q39
H 5.264
4.029
CHROI1ATOGRAI1
1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 3
REPORT HO 136
PKHO
TIME
TOTAL
AREA f1K IDHO
LASCO TUBES
FILE
METHOD
COHC
8
HAME
1
£
3
4
5
6
1.
3.
4.
5.
9.
9.
996
839
029 ;
264
658
957
5747
743
191399 4
6993
83360 1
94751 V
69.
30.
6607
3393
382993
ieo
/if
-------
16:83:2797/95/15
LASCO TUBES
1.9Q9
3.042
==a
\- 5.26
4.828
9.65
CHROhATOGRAII 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE'NO 0
REPORT NO 137
PKNO
£
3
4
5
TIME
1.909
3.042
4.Q28
5.£61
9.65
TOTfiL
AREA MK IDNO
FILE
METHOD
COHC
0
9002
NAME
5699
744
191637
6981
2629
207089
•4
1
98.6427 CSS
1.3573 STYRENE
100
o
to
to
to
w
6
K>
O
IP
-------
3:1697/05/15
1.908
3.044
5. £64
'3.653
1
CHROHATOGRAH i
NO l
SAMPLE NO B
DEPORT HO i;
PKMO TTM:
4.8E9
f1EMORIZED
AREA UK IDMO
I.;,
£
3
c
•J
1.908
3.044
4.029
5.264
5.653
6S03
476
193979
31 £8
465
A
T
1
TOTAL
20484
LASCO TUBES
FILE
METHOD
CQNC
NAME
59.7609 CSS
0.239 STYRENE
100
-------
6'43:0297/05/15
i.048
5.271
6.262
9.65
4.836
LASCO TUBES
ysA
r^m
#
o
t-3
CHROMATOGRAM 1 MEMORIZED
CR501 CHROflATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT NO 139
PKNO
TIME
TOTAL
AREA UK IDNO
1
2
3
4
5
6
1.91S
3.048
4.036
5. £71
6.£6£
9.65 .
S£l£
576
223871
3814
311
576
237361
FILE
METHOD
CONC
9
GG02
NAME
99.7432 CS2
0.2568 STYREME
100
K)
KJ
e
-------
CHROHAT
OGRAM 191 MEMORIZED
57/65/15 17:95:21
LASCO BAG SAMPLES
i— £.787 UlJuJ
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
£
3
CHROMATOPAC
HO £
HO 3
HO 149
TIME AREA 11 K
£.493 53338
£.535 £481 V
£.737 593 V
TOTAL
61403
FILE 9
METHOD 0002
UNO CONC HAME
1 95.9207 METHANE
£ 4.B793 ETHANE
199
2.493
-------
CHRONATQGRAtl 1Q1
37/95/15
MEMORIZED
17:09:15
C . J C'
-------
CHROI1ATOGRAI1 131 MEMORIZED
^7/85/15 17:81:16
p i & O
CR591 CHROHflTOPAC
CHAHMEL MO £
SAMPLE HO 0
;;:PDRT HO 142
LASDO BAG SAMPLES
PKNO
TIME
AREA MK IDMO
FILE
METHOD :
CONC
9
8002
HAHE
1
2
3
2.493
' 2.581
£.788
13751
1573
738
TOTAL
21863
92.2583 METHANE
7.741? ETHANE
188
2.493
tn
H>
to
6
8
u
6
KJ
-------
CHROtlATOGRAtl 101
87/95/19
MEMORIZED
L£:45:BB
LASCQ BAG SAMPLES
|— - £.791
CR501 CHROMATOPAC
CHANHEL HO £
SAMPLE HO 0
REPORT HO 194
F'KNO
1
S
3
CHROHAT
TIME
£.498
£.59
2.791
TOTAL
OGRAM 181
J7/85/19
I '"J 3
AREA HK IBNO
125962 1
5117 V £
1178 V
132189
MEMORIZED
13U£:5E
FILE 9
METHOD B08£
CONC NAME
96.8947 METHANE
3.9B53 ETHANE
188
LASCO BAG SAMPLES
h— • 2.793 •..*«
CR5B1
CHANHEL
SAMPLE
REPORT
PKNO
1
2
3
CHROI1ATOPAC
HO £
NO 0
HO 195
TIME
2.499
2.592
2.793
AREA MK IDHO
126728 1
5169 V 2
1178 V
FILE 9
METHOD 8882
CONC NAME
96.8813 METHANE
3.9187 ETHANE
2.498
2.499
I
6
I-O
TOTAL
133866
iee
-------
;HRQMATOGRAM 101
07/65/19
MEMORIZED
13:32:53
LASCO EAG SAMPLES
1.5Q2
CR5G1 CHROMATOPAC
CHANNEL NO 2
SAMPLE MO 9
REPORT MO 196
FILE
METHOD
)£
PKHO
TIME
AREA UK IDMO
CONC
NAME
1
£
3
2.502
93
c. j
2.796
18342
1049 V
181 V
94
5393
5. 4106
METHANE
ETHANE
TOTAL
CHROMATOGRAtl 101
37/05/19
19572
HEI10RIZED
13:48:02
190
LASCO BAG SAMPLES
2.592
CR5B1 CHRQHATOPAC
CHANNEL HO 2
SAMPLE HO 9
REPORT NO 197
FILE
METHOD
9
9062
PKNO
TIME
1
2
.3
2.502
2.593
2.796
16781
962 V
167 '•>
TOTAL
AREA MK IDNO
1
2
17918
COHC
NAME
94.5774 METHANE
5.4E25 ETHANE
198
o
-P*
-------
CHROMA!
CR5B1
CHANNEL
SAMPLE
REPORT
PKNO
1
2
OGRAH
??/65/
181 MEMORIZED
19 14:07:35
| - £.795 U"J7"
CHROMATOPAC
MO E
HO 8
HO 199
TIME AREA MK IDNO
2.581 117354 1
2.593 4805 V £'
LASCO BAG SAMPLES
FILE 9
METHOD 0002
CONC NAHE
96.0663 METHANE
3.9337 ETHANE
2.501
E.795
1£49 V
CHROI1AT
TOTAL
OGRAM 181
97/85/19
1E348S
MEMORIZED
14U4S58
100
LftSCO BAG SAMPLES
8. 796
2.503
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE MO 8
REPORT MO 280
PKMO
TIME
TOTAL
AREA t1K IDNO
FILE
METHOD
CONC
9
8082
125484
NAME
1
2
3
2.583
2.595
2.796
119232
4897
1275
V
V
1
2
96.Q546
3.9454
180
o
-------
CHRQI1ATOGRAM 181
97/85/19
MEMORIZED
I4:es:83
LASCO BAG SAMPLES
6
KJ
o
F
2.5G2
CR5Q1 CHROtlATOPAC
CHANNEL MO 2
SAMPLE MO 8
REPORT MO £81
FILE
METHOD
9
8882
PKNO
TII1E
AREA UK I DUO
COMC
MAME
1
£
O
2.
2.
2.
582
593
796
22818
1261
331
V
M
1
£
94
5
.7615
.2385
TOTAL
CHROMATOGRAI1 1G1
^7/85/19
24461
MEMORIZED-
14:27:28
£. ?
108
LASCO BAG SAMPLES
2.586
CR5B1 CHROMATOPAC
CHAHMEL MO £
SAMPLE NO 8
REPORT HO £82
FILE
METHOD
PKNO
TIME
AREA tIK IDNO
COMC
MAME
1
£
2.506
2.597
2.792
24508
1319 V
406 V
1
2
94.8925 METHANE
5.1075 ETHANE
TOTAL
26225
108
-------
LftSCO BAG
f—-^ £.797
CR5B1 CHROHftTOPflC
CHANNEL HO £
3AHPLE HO 8
REPORT HO £06
FILE
METHOD
OP£H
9
BOB2
2.593
CJ
6
8
CJ
6
hO
PKNO
TIHE
AREA MK IDMO
COHC
NflflE
£
3
£.503
£.595
£.797
182146
4098
979
V
1
£
96. 1426
3.8574
TOTAL
107££4
1S9
-------
CHROMATOGRAM 181 MEMORIZED ft
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
£
3
37/65/19 16: £4:02
| £.798
CHROtlATOPAC
HO £
NO 8
NO £18
TIME AREA UK
£.504 182868
£.596 4115 V
£.793 967
TOTAL 187954
LASCO BAG SAMPLES ^
FILE 9
METHOD 8682
IDNO CONC NAME
1 96. 1503 METHANE
£ 3.8498 ETHANE
188
CHROMATOGRAM 101 MEMORIZED
(37/85/19 16:31:56
LASCO BAG SAMPLES
WARNING HO PEAK
CHROHATOGRAM 181
4&N*
Z4 ^
1
2.584
NJ
Is)
U>
W
N4
6
K)
MEMORIZED
WARNING HO PEAK
-------
CHROMATOGRAM 1G1
37/05/19
MEMORIZED
16:37:48
LfiSCO BAG SAMPLES
to
2.522
CR501 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO 9
REPORT HO 211
PKNO
1
2
2
4
5
TIME
1.404
. 1.456
2.522
2.613
2.815
AREA
663
1374
13822
745
126
UK
V
V
IDNO
1
£
FILE
METHOD
COHC
9
0002
NAME
94.883 METHAHE
5.117 E.THANE
TOTAL
16729
180
-------
;-IF
. 9 f 7
CR5S1 CHROHATOPAC
CHANNEL MO 2
SAMPLE HO i
REPORT HO 216
FILE
METHOD
9
8982
PKNO
1
2
3
TIME
2.49?
2.588
2.79
AREA MK IDMO
34288
3454 V
16654 V
CONG
NAME
96.8639 METHANE
3.9361 ETHANE
-------
3 ( f t" D / 1
LASCO BAG SAMPLES
CR5Q1 CHROI1ATOPAC
CHANMEL HO £
SAMPLE HO 0
REPORT HO 218
PKNO
1
2
3
TIME
2.49
2.581
2.782
TOTAL
AREA UK IDMO
78495
323Q V
15511 V
97146
1
£
FILE
METHOD
CONC
9
GQ0E
NAME
96.0435 METHANE
3.9565 ETHAHE
100
/ft1/
-------
TOTAL
'37/05/19
126443b
18:32:19
C •
-------
TOTAL
4921430
18:52:39
196
LASCO BAG
SAMPLES
10
o
U)
VI
6
£.788
!.494
CR5Q1 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO 8
REPORT MO £22
FILE
METHOD
9
0882
PKNO TIME
1
£
3
CHROMAT
2.494
2.585
2.788
TOTAL
OGRAM 191
37/05/19
AREA MK IDNO
16205 1
895 V £
11603 V
£3703
MEMORIZED
19:01:49
CONC
NAME
94.7689 METHANE
5.2311 ETHANE
100
LASCO BAG
SAMPLES
}0
CR5Q1 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 9
REPORT NO 223
PKNO
TIME
AREA UK IDNO
FILE
METHOD
CONC
9
0002
1
2
3
2.498
2.587
2.788
TOTAL
CHROMATOGRAM 101
16410
993 V
13096
39409
MEMORIZED
94.7831
5.2169
NAME
METHANE
ETHANE
•I
I
f
-------
CHROMATOGRAM 101
57/85/19
MEMORIZED
19:55:38
£.785
LASCO BAG SAMPLES
2.491
CR5D1 CHROHATOPAC
CHANNEL NO £
SAMPLE NO 0
REPORT NO £38
FILE
METHOD
9
0002
PKNO
TIME
AREA 11 K IDNO
TOTAL 112280
CHROMATOGRAM 101 MEMORIZED
37/95/19 £0:00:10
CONC
NAME
1
c'
3
\ 2; 4 93
1 O . .-.
£';583': <:.
2.735
106894
4370
1016
V
1 l
1
.-,
c
96.8721
3.9£78
188
LASCO BAG SAMPLES
y
2.492
o
01
NJ
N)
bJ
6
w
§
CR561 CHROHflTOPftC
CHANNEL NO £
SAMPLE NO 0
REPORT NO £31
FILE
METHOD
00Q£
PKNO
1
2
3
TIME
2.492
£.584
2.785
AREA
184139
4261
985
UK
V
V
IDNO
1
£
CONC
96.0693
3.9307
TOTAL
189335
NAME
108
-------
CHROflATOGRftH 101 MEMORIZED
£0:12:34
LASCO BAG SAMPLES
,
C6&-
2.491
CR581 CHROMATOPAC
CHAMMEL HO 2
SAMPLE HO 0
REPORT MO £32
FILE
tIETHOD
9
8BB2
PKNO
TIHE
AREA UK IDNO
CONC
NAME
1 2.491
2 2.582
3 2.734
TOTAL
CHROMATOGRAM 181
97/Q5/19
25129
1362 V
276 V
26767
MEMORIZED
£0:17:12
1 94.8572 METHANE
£ 5.1
190
LASCO BAG
428 ETHAME
SAMPLES
\p
2.491
CR5G1 CHROMATOPAC
CHANNEL HO 2
FILE
SAMPLE MO
REPORT MO
£33
METHOD
0G82
o
•31
o
PKMO
TIME
TOTAL
AREA MK IDNO
24715
COMC
NAME
1
2
3
2.491
2. 582
2.784
23282
1251
262
V
V
1
2 .
94.8847
5.1153
108
to
NJ
U)
6
8
-------
CHROtlATOGRAM 181 MEMORIZED
27/85/19 £3:26:41
£.784
LASCO BAG SAMPLES
cbtf
2.491
CR581 CHROtlATOPAC
CHANNEL HO £
SAMPLE: HO e
REPORT HO £34
PKNO
T.I ME
AREA UK IDNO
FILE
METHOD
COHC
9
. GQQc
NAME
1 2.491
2 £.583
3
2.784
TOTAL
CHROMATOGRAM 181
^7/85/1 9
192698
4163 V
969 V
107739
MEMORIZED
£0:34: £6
1 - '' C • f .
. ' i • •
V •
v,, -
1 96
£ 3
18G
LASCO B
.1814 METHANE
.8986 ETHAHE
AG SAMPLES
£.786
2.493
CR581 CHROMATOPAC
CHftMHEL HO £
SAMPLE NO 8
REPORT HO 235
PKHO
1
o
TIME
£.493
£.585
2.786
AREA t1K IDNO
105189
4249 V
981
1
£
FILE
METHOD
CONC
800°
tic.
NftttE
96.1176 METHANE
3.8824 ETHAHE
TOTAL
110418
109
-------
2.785
2.493
o
en
CR5G1 CHROMATOPAC
CHANNEL NO £
SAMPLE MO 0
REPORT NO £36
PKNO
£
TIME
£.493
£.584
£.786
AREA UK IDNO
£4219
1£80
£96
v
a
1
E
FILE
METHOD
CONC
9
8G02
NAME
N)
fy)
04
94.9786 METHANE
5.Q214 ETHANE
TOTAL
£5739
190
-------
CHROMATOGRAH 10:
37/85/19
MEMORIZED
£0:43:50
LASCO BAG SAMPLES
}0
2.494
CR581 CHROnATOPAC
CHANNEL MO £
SAMPLE NO 0
REPORT NO 237
PKMO
1
£
o
TltlE
AREA UK IDMO
FILE
METHOD
COHC
3
QQ02
NAME
2.494
£.585
2.737
TOTAL
21997
1149
249
23395
V
v
•CHROMATOGRftM 1
WARNING HO PEAK
97/05/1/9
HEHORIZED
£B:50:
95.0377 METHANE
4.962S ETHANE
198
LASCO TUBES
LASCO BAG SAMPLES
2.491
CR5G1 CHROMftTOPflC
CHAHMEL 110
SAMPLE NO
REPORT NO
PKMO
c
0
£38
TIME
1
2
3
2.491
2.582
2.784
28508
1889 V
225
TOTAL
AREA UK IDNO
1
£
FILE
METHOD
CONC
9
0002
21885
NAME
94.9931 METHANE
5.0069 ETHAME
108
-------
2.499
CR5G1 CHROHftTQPAC
CHANNEL HO £
SAI1PLE NO 9
REPORT NO 37
PKHO
TIME
AREA !1K IDNO
FILE
METHOD
CONC
y
8882
NAME
3.794
TOTAL
!680£
1316 V
476 V
18589
92.7344 METHANE
7.£656 ETHANE
168
ot
-------
I LMHL
37/85/22
16:03:49
LASCO BAG SAtlPLLb
Ju-J
:.496
CR5B1 CHROPIATOPAC
CHANNEL HO 2
SARPLE MO 0
REPORT MO 34
PKHO
1
£
TIME
2.496
2.585
2.79
AREA MK IDHO
16963 1
1346 V £
475 V
FILE
METHOD
COMC
HAME
92.6598 I1ETHAHE
7.3492 ETHANE
-------
£.79
L. * %/ V
2.497
CR581 CHRQttATOPAC
CHANNEL HO 2
SAMPLE NO 8
REPORT HO 38
PKNO
1
2
3
TIHE
2.497
2.588
2.79
AREA HK IDNO
FILE
METHOD
COHC
9
9882
NAME
91681
3571 V
880 V
96.2588 METHANE
3.7492 ETHAME
-------
TOTAL
97/65/22
939236
14:59:24
2.796
1G8 .
LASCO BAG iSAMPLES
2.581
CR5B1 CHROI1ATOPAC
CHANNEL NO 2
SAMPLE NO
REPORT NO
0
28
FILE
METHOD
9
OG02
PKMO
TIME
2.501
•2.594
2.796
AREA MK
90911
3691 V
794 V
IDHO
1
COMC
MfiHE
96.1S95 METHANE
3.8185 ETHANE
TOTAL
95306
1 Ofl
-------
CHROMAT
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
£
A
TOTAL 107584
0GRAM 101 MEMORIZED
17/05/22 11:48U1
CHROtlATOPAC
NO 2
NO O
NO 17
TIME AREA MK
2.439 19737
2.578 I486 V
£.781 681 V
100
LASCO BAG SAMPLES
FILE 9-
METHOD S8i2
IBNO CONC NAME
1 93. 3484 METHANE
£ 6.6516 ETHANE
TOTAL £18£5
;HROMATOGRAM 101 MEMORIZED
2 11:52:41
188
LASCO BAG SAMPLES
£.489
2.78!'
2.489
CR501 CHROtlATOPAC
CHANNEL NO £
FILE
SAMPLE HO
REPORT NO
PKNO
0
18
TIME
1 2.489
£ 2.578
3 2.781
AREA MK IDNO
1
28239
1429 V
668 V
£
flETHOD
CONC
8002
NAME
93.4063 METHANE
6.5932 ETHANE
K>
cn
TOTAL
22336
109
-------
CHROMATOGRAM 101
27/65/22
MEMORIZED
11:39:35
2.78
LASCO BAG;SAMPLES
2.488
CR5B1 CHROMATOPAC
CHANNEL MO £
SAMPLE HO 8
REPORT HO 15
FILE
METHOD
PKNQ
3
TIME
AREA UK IDHO
TOTAL 186633
;:HRDMATOGRAt1 101 MEMORIZED
37/05/22 11:43:59
COMC
NAME
2.
£.
2.
488
579
73
101712
3971
950
w
V ...
1
c.'
96.
^,
O •
2422
7578
£.783
190
LASCO BAG SAMPLES
N3
Ol
K3
6
VI
S
2.489
CR501 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO 0
REPORT HO 16
PKNO
TIME
AREA MK IBHO
1
£
3
2.489
2.581
2.733
102614
4G11
959
V
V
1
2
FILE
METHOD
COHC
9
000£
NAME
96.2381 METHANE
3.7619 ETHANE
L
-------
CR501
CHANN
SAMPLE NO
REPORT HO 13
QGRAfl 181 MEMORIZED
37/B5/2E 115 15: 19
I
CHROMATOPAC
NO £
NO 9
LASCO BAG SAMPLES
C. * *J f O
FILE 9
METHOD Q802
PKHO
1
E
ntiE
2.486
2.578
AREA UK IDNO
COHC
NAME
16365
687B V
TOTAL £2435
CHROMATOGRAH 181 MEMORIZED
97/65/22 ll:£3:£3
1
£
72.9448 METHANE
E7.Q55E ETHANE
180
LASCO BAG SAMPLES
2.486
2.435
CR501 CHROMATOPAC
CHANNEL NO 2
SAMPLE HO 0
REPORT HO 14
PKHO
1
£
TIME
2.485
£.577
AREA fit
15413
5751 V
IDNO
1
£
FILE
METHOD
CONC
NAME
72.3251 METHANE
£7. 1749 ETHANE
TOTAL
£1164
160
-------
;HROMATOGRAM 101
97/65/22
MEMORIZED
1B:49:11
LASCO BAG SAMPLES
£.433
CR561 CHROMATOPAC
CHANNEL MO 2
SAMPLE HO O
REPORT HO 11
>KNO
1
£
TIflE
2.483
£.574
AREA UK IDNO
55987
3381
TOTAL 59288
CHROMATOGRAM 101 MEMORIZED
97/05/22 10:55:33
FILE
METHOD
COHC
0002
NAME
94.4324 METHANE
5.5676 ETHAHE
100
LASCO BAG SAMPLES
£.483
CR5Q1 CHROMATOPAC
CHAHMEL MO 2
SAMPLE HO 9
FILE
METHOD
9
00S£
REPORT HO 12
PKHO TIME
1
£
2.483
2.575
TOTAL
AREA UK IDNO
56299
3313 V
5961£
1
2
CONC
NAME
94.4432 METHANE
5.5568 ETHAHE
100
to
ll
-------
?7/85/22 10:31:50
2,775
LASCO BAG SAMPLES
•9-M '
8.483
CR561 CHROI1ATOPAC
CHANNEL NO 2
SAMPLE NO 8
REPORT NO 9
FILE
METHOD
9
088£
PKMO
' TIME
AREA MK IDNO
TOTAL 109231
CHROMATQGRAN 101 MEMORIZED
37/05/2S 10:38:83
COMC
HAttE
1
£
.*,
o
2.483
2.575 '
2.775
163959
4216
1857
1
y 2
1 1
V
96. 1023
3.8972
i
p-2.777U'V"
100
LASCO BAG SAMPLES
to
w
6
S
2.484
CR581 CHRQHATOPAC
CHANNEL NO 2
SAMPLE NO 0
REPORT NO 18
PKMO
TIHE
TOTAL
AREA MK IDNO
FILE
METHOD
CONC
9
0005
48024
NAME
1
2
3
2.484
£.576
2.777
45549
1877
597
V
V
1
2
96.8425
3.9575
188
-------
SAtlPLE MO
REPORT HO
OGRAtl 101 MEMORIZED
57/05/22 18:28:82
| — 2.775"'"
CHROMATOPAC
NO £
NO 8
LASCO BAG SAMPLES
FILE 9
METHOD 8882
2.484
PKNO
TIHE
AREA HK IDNO
CONC
NAME
.1
2
3
CHROMAT
CR501
CHANNEL
SAMPLE
2.434
2.573
£.776
TOTAL
OGRAtl 101
37/85/22
CHROMATQPAC
NO £
NO 8
18811
1478 V
674 V
28963
MEMORIZED
18: £5: 16
1 92.7172 METHANE
2 7.2828 ETHANE
100
LASCO BAG. SAMPLES
FILE 9
METHOD 8882
2.484
REPORT MO 8
PKMO
TIME
AREA MK IDNO
CONC
NAME
1
£
3
2.484
£.573
2.776
18879
1477
672
V
V
1
o
L.
92.743
7. £57
TOTAL 21028
CHROhATOGRAH 181 MEMORIZED
196
-------
TOTftL
;HROMATOGRAM 101
37/65/22
£17850
MEMORIZED
18:06:09.
190
LASCO BAG SAMPLES
2.432
CR5B1 CHROMftTOPftC
CHANNEL NO £
SAMPLE NO 6
REPORT NO 5
PKNO
TIME
AREA UK IDNO
FILE
METHOD
CONC
9
8002
NAME
1 £.482
2 .2.573
TOTAL .
CHROMATOGRAM 101
37/05/22
£4473
4479 V
28952
MEMORIZED
10: 12:34
1 84.5306
2 15.4694
100
METHANE
ETHANE
LASCO BAG SAMPLES
2.482
CR501 CHROI1ATOPAC
CHANNEL NO 2
SAMPLE NO 8
REPORT NO 6
FILE
METHOD
9
0002
to
PKNO
1
2
TIME
2.482
2.572
AREA UK IDNO
23572
4290
1
2
CONC
NAME
84.6Q29 METHANE
15.3971 ETHANE
TOTAL
27862
1D0
-------
CHROMATOGRAM 181
37/95/22
MEMORIZED
09:45:46
LASCO BAG SAMPLES
r
i,36-§
CR5G1 CHROI1ATOPAC
CHANNEL HO 2
SAMPLE NO 0
REPORT NO 3
FILE
METHOD
9
0B0S
to
PKNO
1
£
' TIME
2.479
£.51
66
AREA UK IDNO
156054
53094
V
£ TOTAL • . 2B914S
CHROMATOGRAM 1B1 MEMORIZED
37/85/22 89:53:38
f
COHC
HAME
74.6142 METHANE
25.3858 ETHANE
. 100
LASCO BAG SAMPLES
KJ
N>
U)
6
Sib
iitfi
CR501 CHROMATOPAC
CHANNEL NO 2
SAMPLE MO O
REPORT NO 4
PKMO
1
TIME
£.481
£.573
AREA UK IDNO
16£487
55363
1
£
FILE
METHOD
COHC
9
90ee
NAME
h
I
74.5868 METHANE
25.413£ ETHANE
-------
CHROMATOGRAM 1 MEMORIZED
WARNING NO PEAK
CHROMATOGRAM 1Q1 MEMORIZED
CR5B1
CHANNEL
SAMPLE
REPORT
?7/95/££ 89: £8: 35
CHROMATOPAC
HO £
MO 8
NO 1
PKMO TIME AREA MK
1
2.475 15477
TOTAL 15477
CHROMATOGRAM 101 MEMORIZED
J7/95/22 89: £9: 86
i
CR591
CHANNEL
SAMPLE
REPORT
CHROMATOPAC
. HO £
MO 8
HO 2
PKNO TIME AREA MK
1
2.48 15535
TOTAL 15535
LASCO BAG SAMPLES
FILE 9
METHOD 0882
I DM0 CONC NAME
1 100 METHANE
168
LASCO BAG 'SAMPLES
FILE 9
METHOD 0802
I UNO CQNC NAME
1 100 METHAHE
109
2.475
2.48
-------
1
CR501
CHANNEL
SAMPLE
REPORT
PKHO
1
£
3
i
CHROMATOPAC
HO 2
HO Q
HO 48
TIHE
2.496
£.585
2.788
AREA UK
18982
1273 V
13322
FILE 9
METHOD OOG2
IBNO CONC NAME
1 93.7146 METHANE
Z 6.2854 ETHAME
TOTAL
33577
190
4
I
1
-------
CR581
CHANNEL
SAMPLE
REPORT
PKHO
1
£
3
i
CHROMATOPAC
NO £
HO 8
HO 47
TIHE
3. 497
2.587
2.791
AREA HK
19983
1£8£ V
1346S
TILE 9
I1ETHOD 0ei£
IDHO CONC HAME
1 93.7842 METHANE
2 6. £958 ETHANE
8.791
TOTAL 33767
CHRQtlATQGRAn 101 HEHORIZEB
100
-------
CR581
CHANNEL
SAMPLE
REPORT
P.KHO
1
2
o
w
37/65/22
r
CHROHATOPAC
HO £
NO 8
NO 46
TIME
2.498
2.589
2.791
TOTAL
CBROMATQGRAM 181
£1:32; 97
AREA MK
68892
2472 V
31281 V
94565
MEMORIZED
LASCO BAG SAMPLES
FILE 9
METHOD Q8B2
IDHO COMC NAI1E
1 96.8984 METHANE
2 3.9816 ETHANE
100
-------
1
I
1
CR5Q1
CHANNEL
SAMPLE
REPORT
PKI10
1
^
3
CHROMA'
r
CHROMATOPAC
MO £
MO 0
MO 45
TIME
2.498
2.59
2.793
TOTAL
IOGRAM 191
AREA MK
5999Q
£438 V
32191 V
93621
MEMORIZED
FILE 9
METHOD 9002
IDHO COHC NAME
1 96.0506 METHANE
£ 3.9494 ETHAhE
109
:
2.49(
2.79:
0)
00
N)
to
OJ
I
-------
CR501 CHROflATOPAC
CHANNEL MO 2
SftHPLE NO 8
REPORT NO 43
PKNO
1
HUE
S.499
FILE
METHOD
9
8882
AREfl MK JBNO
11844 1
CONC NAME
93.8524 METHflME
KJ
W
OJ
6
i
£.59
2.794
723
286
6.1476 ETHANE
TOTAL
11967
188
-------
97/05/22 80:55:18
LASCO BAG SAMPLES
2.499
CR501 CHROMATOPAC
CHANNEL NO 2
SAMPLE NO
REPORT NO
PKNO
1
2,
3
e
42
TIME
2.499
2.589
2.793
AREA MK IDHO
11779
777 V
£13
1
E
FILE
METHOD
GONG
9
8982
NAME
93.8885 METHANE
6. 1915 ETHANE
TOTAL 12769
CHROHATOGRAM 181 MEMORIZED
180
-------
•»7/85/££ £9:47:52
LASCO BAG SAMPLES
2.498
CR5Q1 CHROflATOPAC
CHANNEL HO £
SAMPLE NO 0
REPORT HO 41
F'KHO
TIME
1
J^
•3
£.498
• £.588
£.783
1£469
824
£48
V
M
AREA UK IDNO
1
TOTAL 13532
CHROI1ATOGRAI1 181 MEMORIZED
£
FILE
METHOD
CONC
NAME
93.8044 METHANE
6.1956 ETHANE
100
-------
9.7/85/££ £8:38:33
LASCO BAG SAMPLES
F
3.498
CR5Q1 CHROflATQPAC
CHANNEL NO £
SAMPLE NO S
REPORT NO 48
PKNO
1
3
TIME
2.498
2.59
8.79£
AREA UK IDNO
FILE
METHOD
CONC
NAME
3285Q
1455 V
£84 V
£
95.7582 METHANE
4.£418 ETHANE
CJ
6
6
SJ 1
TOTAL
CHROHATOGRAD 1Q1
34589
HEflORIZEB
tee
-------
37/05/22 £0;32:14
F
LASCO BAG SAMPLES
:.499
CR561 CHRQMATOPAC
CHANNEL MO £
SAMPLE HO 8
REPORT NO 39
PKNO
TIflE
I 2.499
2 £.592
3 2.794
TOTAL
CHROHATQGRAH 101
AREA MK IDNO
FILE
METHOD
COMC
9
998£
37£34
1647
39194
MEMORIZED
£
NAME
95.764 METHANE
4.2359 ETHANE
168
-------
VI
6
;HRQt1ATOGRAI1 181 MEMORIZED
£ £B:££:£8
F27794u*°-'
LftSCO BAG SAMPLES
9-9-1
2.499
CR5B1 ' CHROMATOPAC
CHANNEL HO £
SAMPLE HO 9
REPORT HO
33
FILE
METHOD
9
8862
PKHO
TII1E
AREA MK IDHO
COHC
HA HE
1
2
3
£.499
£.592
2.794
48419
1799 V
347 '•/
1
i-,
C
95.7532 METHANE
4.£418 ETHAHE
TOTAL 42556
CHROHATOGRAil 101 MEMORIZED
100
,J
-------
1849/ SI74 BYTES USED
38: £5:
5/2//97 LASCO TUBES
& IS A*
1.873
£.975
=3
5.287
3.973
CHROMATOGRAN 1 MEMORIZED
CR5G1 CHROI1ATOPAC
CHANNEL HO 1
SAMPLE HO 9
REPORT HO £
TILE
METHOD
0
906£
PKNO
1
O
l_
3
TIME
1.873
£.975
3.978
AREA
171S
874
221136
COHC
NAME
5.3155 CSS
4
5
6
7
n
O
9
10
5.207
6 « 36 c!
9.59
19.067
18.367
10.458
10.767
4656
73547Q
1671766
1531362 V
185
466 V
590
3
1
•^
L.
17.6736 UNA
40.1844 STYRENE
36.8215 CUMEME
o
•Q
(O
TOTAL
4168708
i n n
-------
LM3CU I U C L O
1.881
£.983
~ >
5.£12
6.£0£
to
to
6
8
CHROHATOGRAH 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT NO 3
PKNO
TIME
AREA MK IDNO
FILE
METHOD
CONC
G
G002
NAME
H
£
3
4
5
6
7
3
g
1.881
£.983
3.985
5.212
6.£0£
b.Sbb
9.595
10.074
18.775
1688
868
£££!£?
468£
£85
732471
163992G
1500336
. 6£9
o
1
£
5.4£57 CS£
17.8915 HMA
40.0351 STYRENE
36.6476 CUMEI1E
TOTAL 4102106
•18:53:1697/05/21
CHROMATOGRAM 1 MEMORIZED
"^NTNll NO
.100
LASCO TUBES
-------
6:55:3897/95/21
LASCO TUBES
;- 3 Q 4.
I— • ^ ,- ~
5.218
6.2S8
-6,874
3,988
IB-.Kl
CHROHATQGRAH 1 'MEMORIZED
CR501 CHROMATQPAC
CHANNEL HO 1
SAHPLE NO 8
FILE
nETHOB
8
BBB2
REPORT
F'KHO
i
2
3
4
5
6
7
8
HO
4
TIME
2.
3.
5.
6.
6.
9.
18.
18.
994
988
218
288
874
6
879
549
AREA I11C IDHO CONC
1291
228490 4
2878
276
21979 3
197782 1
471 S
5827
NAME
58.8304 CS2
4.985 HflA
44.8778 STYREHE
9.1868 CUMEME
o
CO
ro
is)
-------
18B
i • I 3 i O D 7 f ' I
£.999
:.'" in
5. £17
• 6. £14
6.88
ie.B7rw
CHROHATDGRAH 1
CR5B1 CHROMATOPAC
CHANNEL NO 1
SAHPLE NO Q
REPORT NO. 5
PKNO TIME
1 2.999
2 3.995
3 5.217
4- 6.214
5 6.88
6 9.6Q5
7 18.675
.' 3 ' C I
3.995
MEMORIZED
AREA UK
1276
219319
2882
£78
22108
260156
993
LHbLU lUCtS
FILE 8
METHOD B0B2
IDHO COMC NAME
4 49.55*5.1 CS£
:ilt'.
3 4.9953 MMft
1 45.££5£ STYRENE
2 8.2244 CUME11E
C4E-S-1
Fff ft
6
ro
O
TOTAL
447012
108
-------
Hi
3.995
5. ££7
6. £15
6.882
60S
CHROMATOGRAM
1 MEMORIZED
CR5BI CHROMATOPAC
CHANNEL HO 1
SAMPLE NO 8
FILE
METHOD
0
B062
REPORT;
PKNO
1
£
3
4
5
6
7
8
9
10
11
NO 6
v,. TIME
1.376
1.575
1.879
2.132
3.015
3.417
3.995
5.227
6. £15
6.882
9.608
TOTAL
AREA
825
7473
2588
£608
2111
105£
££1948
3956
6££
1983
£6737
£71904
I UNO
CQNC
NAME
o
CO
88.5426 CS2
0.791 MHfl
10.6664 3TYRENE
100
K)
K)
U
6
3
u
VI
6
-------
ll.'56:3897/85/£l
F SSfll
LASCO TUBES
-5-/
4.0G5
5. £38
6. £17
MSI
4-615
CHROMATOGRAM. 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 6
REPORT NO 7
PKNO
3
4
5
6
7
8
9
19
11
12
TIME
1,
1,
1,
2.
3,
3.
4,
5,
6,
6.
7,
q
377
577
881
136
0££
425
005
£38
£17
883
434
615
AREA MK IDNO
994
8961
3089
3086 V
£518
1245
243732 4
4673
741
2369 3
343
3£140 1
FILE
METHOD
CONC
0
000£
NAME
87.5975 CS2
0.8513 MMA
11.5512 STYREHE
-------
TOTAL. 3Q3891
£:i7U797/05/21
1.577
3.603
iee
LASCO TUBES
AF'5'2
A
4.887
5. £39
6. 23
J-l f <-l",
CHROMATOGRAH 1 MEMORIZED
CR5Q1 CHRQilATOPfiC
CHANNEL NO 1
SfttlPLE HO 8
REPORT NO 8
PKNO
TIME
v AREA MK ID NO
FILE
METHOD
CONC
Q
0B8S
NAME
o
^fl
01
1
e
5
6
7
8
5,
6,
6,
9,
577
803
007
,239
,23
,895
,6££
18,898
622
5429
£19498
3402
£99
45897
3£7598
642
1
e
36.9744 CS2
7.7317 MHA
55.1858 STYRENE
0.1882 CUMEME
K>
*°l
6
|
6
10
-------
TOTAL 663380
12:37:5897/95/21
188
LASCO TUBES
1.581
3.009
— •-*
5.244
6.234
fti
4.011
10.TOT"
CHROHftTDGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL MO 1
SAMPLE NO 8
REPORT MO- 9
PKNO
TIME
AREA UK IDM0
FILE
METHOD
CONC
0
0002
MAME
1
£
3
4
5
6
7
8
1.5S1
3.089
4.611
5. £44
6. £34
6. 896
9.625
10.10?
621
5335
£15434
3318
289
446E4
317893
624
1 7 O (I f I 7
:• I . I. t t' t
7.71E
54.9394
nun
STYRENE
0. 1B78 CUMEME
-------
TOTAL 588188
2:59:0197/65/21
3.91
5. £46
6. £35
G.OQ8
10.104
4.015
180
LASCQ TUBES
A&-S-2,
l\
CHROHATOGRAM 1 MEMORIZED
CR501 CHRQNATOPAC
CHANNEL MO 1
SAMPLE HO 8
REPORT MO 19
PKHO
TIME
AREA t1K IDHO
FILE
METHOD
COHC
Q
0Q 8 £
o
••o
NAME
1
e
3
4
5
6
7
3
9
1.531
1.9
3.01
4.015
5.246
6.235
6.898
9.624
10. 104
838
351
6478
£54701
4836
379
55945
724851
1168
£4.5693 CS2
5.3966 MMA
69.3215 STYREHE
9.1126 CUMEHE
Kl
ro
s
I
&
-------
I
-------
TOTAL 794346
100
: o • H i ; j i ? f i \
r 3.889
==—
5.245
6. £36
««•— tr Q
V .-.-„-
CHROHATQGRAtt 1
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE MO' 0
REPORT HO 12
PKHO TIME
1 3.809
£ 4.012
3 5.245
4 6.236
5 6.9
6 9.b£8
7 9.978
1" J * C. i
4.012
(1EHORIZED
AREA UK
8£97
£07281
3100
£77
31733
264928
54693 V
LHSLU IUCL5
FILE Q
METHOD 8802
I.DHO COHC MAME
4 41.131'S GS2
3 6. £96 9 MMA
1 52.5713 STYRE
o
'.O
--3
6
£
6
SI
'0-5O-
-------
3.019
5.256
6.247
-4.912
4.819
CHROHATOGRAH 1 MEMORIZED
CR5B1 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO 14
PKNO
1
£
3
4
5
6
7
TIHE
FILE
e
6802
AREA •MK IDHO
COMC
HA HE
o
(O
CO
3.819
4.819
5.256
6.247
6.912
9.64
9.944
3776
287175
2953
277
31127
274446
423S8 V
TOTAL
562143
40.4048 CS2
6.9706 Mdft
53.5S46 STVREHE
188
to
to
XI
-------
1 «r . If « LO?f
• 3.821
:: s=s=*—
5.257
6. £49
— -6-. 913
I... a. if, in
'OJ/CA LHSUU TUBES
- 4.822
CHROHflTOGRflH 1 MEMORIZED
CR581 CHROMflTOPftC
CHANNEL NO 1
SAMPLE HO B
REPORT NO 15
FILE
METHOD
PKNO
1
£
3 .,
4 '"
5
6
TIME
3.821
4.822
5.257
6. £49
6.913
9.648
AREA
3966
£12787
3133
291
33191
256896
TOTAL
518265
o
1
CONC
NAME
42.3142 CS2
6.6883 MMA
51.0855 STYREME
IBB
-------
CHROMAT
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
2
3
4
5
6
7
8
9
10
11
12
ii?ii
3.Q33
.
• 5.26
6. £42
- 6.916
1 ft 'J Qlff f A
\ 1 M m ft A 0
1 iOIOiO
OGRAI1 1
CHROHATOPAC
HO 1
HO 3 V-.'
NO 16 »*'•
TU1E
1.589
1.9S4
2.142
3.033
4.924
5.26
6. £42
6.916
9.392
9.646
18.444
10.613
4.824
MEMORIZED
AREA UK
1863
662
475 V
1166
289743
3497
387
12347
286
453303
661
536 V
UHS^U 1 UBLO
;
FILE 0
riETHOD BBBS
1DNO CONC NAME
4 31.8549 CS2
3 1.8281 MtlA
1 67.117 STYRENE
10-5-2
o
10
S3
to
U)
6
KJ
O
oo
SI
6
TOTAL
684926
-------
5:31:4497/05/21
LASCO TUBES
10-5-
3.025
5. £63
6.£55
6.92
Q A ft (.
4.Q27
\ 18.433"
CHROI1ATOGRAM 1
flEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKMO
1
£
•~\
•J
4
5
6
7
8
9
10
11
CHROMATOPAC
MO 1
MO O
HO 17
TIME
1.59
1.904
2.154
3.025
4.027
5.263
6.255
6.92
9.466
9.648
18.433
AREA MK IDHO
1793
644
466 V
1157
£08191 4
3508
383
12389 3
£73
454380 1
677
FILE
METHOD
CDNC
O
0802
NAME
30.845 CSS
1.8355 MHA
67.3195 STYREME
-------
TOTAL 683855
15:54:0497/85/21
199
LASCO TUBES
4.023
5.255
6.249
6.988
9.645
CHROI1ATOGRAM 1
CR501 CHROMATOPAC
CHANNEL MO 1
SAMPLE MO 0
REPORT HO 18
I1EMQRIZED
PKHO
TIME
ftREA UK IDHO
FILE
METHOD
COHC
0
0002
HAME
1
2
3
4
5
6
7
1.907
3.029
3. 735
4.023
5.255
6.249
6.908
469
1425
330
286158
10367
280
535
8
9.645
3369
98.1418 CS2
0.2545 MMA
1.6036 STYREME
to
ro
CJ
Nl
-------
TOTAL 738611
7:01:8297/85/21
100
LASCO TUBES
1 591
I - HI
3.045
5.258
6.£5
h 6.924
4.031
lS:Hi
CHROHATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAHHEL HO 1
SAMPLE HO O
REPORT HO £1
FILE
METHOD
6
0002
PKMO
TIME
AREA t1K IDNO
COHC
HAME
1
^,
c
3
4
5
6
7
8
9
10
11
12
13
391
593
892
845
031
5.258
6.25
6
9
9
10
924
407
652
,125
18.442
138
1455
505
438
785
£06563
2849
389
7173
£71
379165
534
366
34.8081 CS2
1.2087 MMA
63.3933 STYRENE
0.0.9 CUMEHE
TOTAL
600592
i an
-------
TOTAL 213520
6:38:4497/85/21
106
LASCO TUBES
•ill
:!§3
3.Q47
5.269
6.25
h 6.922
lOr -
4.833
CHROHATOGRAI1 1 MEMORIZED
CR581 CHRClMATOPAC
CHANNEL NO 1
SAMPLE NO G
REPORT NO 20
FILE:
METHOD
0
8002
PKND
TIME
AREA HK IDHO
CONG
NAME
1
2
3
4
5
6
7
8
9
10
11
1£
13
14
1.
1.
1.
2.
3.
4.
5.
6.
6.
9.
9.
10.
16.
395
596
965
15
647
033
269
25
922
392
648
13
446
10.616
278
1905
668
651
927
£37847
3651
496
9179
371
481695
639
399
506
32.6372 CS2
1.2596 MMA
66.0156 STYRENE
0.0876 CUMEME
K)
K>
CO
6
to
o
CJ
N4
6
to
-------
TOTAL £££931
16:16:2197/95/21
LASCO TUBES
5.257
6.£53
6.968
4.0S5
9.646
CHROMATOGRAM 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 9
REPORT MO 19
FILE
METHOD
0
0882
PKMO
TIME
AREA MK IDNO
COMC
NAME
1
£
3
4
5
6
7
8
9
1.591
1.911
3.Q31
3.739
4.025
5.£57
6.£53
6.9G8
9.646
£48
454
1374
3£3
202130
9967
£71
515
3188
98.2016 CSS
B.E5 HMA
1.5483 STYRENE
-------
LHbUU lUBLb
1.905
3.025
-
5.26
6.252
4.024
118.833
CHROMATOGRAM 1
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 22
MEMORIZED
PKNO
TIME
AREA MK IDHO
FILE
METHOD
COHC
0
0802
NAME
to
10
OJ
6
to
o
6
S3
1
*-,
c
.-1
-Jl
4
5
6
7
8
9
1.905
3.025s.
4.024 '**
5.26
6.252
6.915
9.645
10.127
10.833
1447
920
'-207124
4505
281
715662
1648994
1514694
979
5.8636 CS2
2
17.5117 M
49.3531 STYREHE
37.D666 CUMEME
TOTAL
4894545
1 Pifl
-------
1.9Q8
3.825
4.G28.
5.26
6.251
I 10.839
CHR8I1ATOGRAM 1
CR591 CHROtlATOPAC
CHANNEL MO 1
SAMPLE NO 0
REPORT NO £3
MEMORIZED
PKNO
TIME
AREA MK IDM0
FILE
METHOD
CONC
8
0002
NAME
I
£
•j
4 ,
5
6
7
8
9
1.998
3.025
4.828
5.26
6.251
6.913
9.642
18. 123
18.839
1423
912
208357
4507
282
717542
1653884
1516798
1092
TOTAL
4184889
1
2
5.0361 CSS
17.5156 MMA
48.3723 STYREHE
37.8259 CUMEME
-------
15:00:2797/95/19
LASCO TUBES
1.908
3.038
4.831
CHROI1ATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAHHEL HO 1
SAMPLE HO 0
REPORT MO 203
PKMO
TIME
TOTAL
AREA UK IBNO
1
£
•J
4
5
6
7
8
9
1.988-
3. 038
4.031
5. £69
6.25
9.241
9.5
9.625
9.781
2389
1016
232035
5290
349
4037
798
1325
789
248023
FILE
METHOD
CONC
0
G082
NAME
KJ
10
CJ
6
KJ
O
9,9.4324 CSS
0.5676 STYREI1E
100
-------
15:24:2297/05/19
LASCO TUBES
1.9Q?
3.QS5
===»
5.£66
4.028
CHROMATOGRAM 1 MEMORIZED
CR581 CHROtlATOPAC
CHANNEL MO 1
SAMPLE MO 0
REPORT MO
2(
PKNO TIME AREA HK IDHO
1 1.907 1592
2 3.025 -761
3 4.028 200308 4
4 5.266 3810
5 10.383 3113
6 10.708 7899 V
TOTAL 217484
FILE
METHOD
COMC
190
O
0002
MAME
CS2
o
100
-------
•j- : 1 J^//t
1.919
3.05
— =— —
C r\ O H
j . c 9 1
6.278
'3/iy LflbUU lUbLb
4.057
L ^'iVaSL-i
r 5 pS.nU'O.L
1 . 10.849
CHROMATOGRAM 1
CR501
CHANNEL
SAMPLE
REPORT
PKHO
1
2
3
4
5
6
f
8
q
10
11
12
13
14
15
CHROMATOPAC
HO 1
HO O
MO 207
TIME
1.919
•V'' .
'• -5
3.05
4.057
5. £91
6.278
6.935
8.75
9.008
9.267
9.442
9.652
9.8
9.968
10. 133
19.349
1 U >J
MEMORIZED
FILE 0
METHOD 0062
AREA UK I DM0 COHC NAME
1446 ' :.:;:'
928
232072 4 15.67 CS2
4936
348
298416 3 £0. 1496 MMA
1147
861
7£5 V
1196 V
418191 V 1 28.2371 STYRENE
1647 V
1367 V
53232S V £ 35.9433 CUMEME
2424
Lou/
TOTAL
1498927
169
-------
17:37:5097/95/19
LASCO TUBES
1.903
3.817
—
5. £56
4.818
01
OJ
CHROMATQGRAM
1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 9
REPORT NO £15
PKNO
TIME
AREA IIK IDNO
FILE
HETHOD
CONC
0
9692
NAME
ro
10
U)
o
OJ
1
£
3
4
5
6
7
8
9
10
11
IS
13
1.993
3.017
4.818
5.256
6.249
6.911
9.276
9.499
9.639
10.12
18.35S
10.525
10.833
1049
699
200563
3724
£66
£24942
1487
1348
313821
402689
1530
996
3817
V
V
V
V
17.5622 CSS
19.6969 I1HA
27.4796 STYRENE
35.2613 CUMEME
TOTAL
1156925
108
-------
TOTAL 184395
108
1 / • -j f • 0 1) y / /
1.898
3.008
• 5. £46
6. £38
U D / 1 y
4.0G8
LflSCU TUBLb
0 A£( (.,...
-• • uf',-|
^ 10.414 iw
CHROMATOGRAH 1
CR5B1
CHANNEL
SAMPLE
REPORT
PKHO
1
£
3
4
5
6
7
3
9
10
CHROMATOPAC
HO 1
HO 0
HO £17
TIME
1.898
3.008
4.808
5. £46
6.238
6.902
9.496
9.63
10.112
10.414
TOTAL
MEMORIZED
AREA UK
1038
716
284590
3861
288
235866
1525
331638
425122
1941
1206576
FILE 0
METHOD 0002
IBNG CQMC MftME
4 17.0883 CS2
3 19.7912 I1MA
1 27.7008 STYRENE
2 35.5892 CUMEHE
100
SJ
N)
CJ
6
ro
O
6
N>
-------
13:£0:4297/05/19
LASCO TUBES
1.902
3.G24
«—
5.249
6.241
6.'J 0
4.013
CHROMATOGRAfl 1 HEHORIZED
CR581 CHROHATOPAC
CHflMMEL NO 1
SAMPLE HO G
REPORT MO £19
PKNO
1
TIME
1.902
3.Q24
4.013
5.249
AREA !1K IDHO
1119
738
206944 4
3943
FILE
METHOD
COMC
0
0002
NAME
16.889 CS2
o
C/l
5
6
7
8
9
10
11
12
13
241
904
982
,307
,634
,775
,117
10.395
10.681
6.
6.
8.
9.
9,
9,
10,
299
238253
6173
11652
347916
11332
432207
2464
1389
V
V
V
V
V
19.444£
28.3939 3TYREHE
35.273 CUMEHE
KJ
U
6
VI
6
10
-------
£8:55:2197/85/19
LASCO TUBES
1.893
3.816
__-j^
5.£44
6.235
4.888
t 11:111
CHROHflTOGRftM 1
CR581 CHROMftTOPAC
CHANNEL HO 1
SAMPLE NO 8
REPORT HO £39
MEMORIZED
KJ
6
I
VI
6
KJ
PKNO
TIME
AREA MK IDNO
FILE
METHOD
CONC
MA ME
i
j-,
c.
3
4
5
6
7
B
•3
10
11
12
1.393
3. 816
\ 4.898 :•
1 ' i;
• , 5. £44 :"
6.235
6.899
8.778
9. £73
9.629
18.11
18.416
18.814
3824
956
284434
5089
£69
719888
2431
10184
1559818
1413539
5141
3361
<;'
y
y
T8TAL
3927158
5.2461 CS£
18.4735 f1MA
48.8Q67 STYREHE
36. £737 CUE1EHE
188
-------
1:1: 16: £197/85/19
LASCO TUBES
1.892
3. 014
—
5.239
4.QG4
iu. iii
CHROHATOGRAtl 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL MO 1
SAMPLE NO 0
REPORT NO £40
PKMO
1
2
o
4
5
6
7
8
9
10
TIME
1.392
3.014
4.084
5.239
6. 397
9.377
9.628
10.111
10.325
10.671
AREA
£837
893
282791
4728
695169
4793
1308366
1377466
£971
6102
Mf
V
y
V
V
FILE
METHOD
CONC
0
0802
NAME
18.3721 nnft
39.364 STYREME
36.4945 CUMEME
11 10.333 542 V
TOTAL 3896648
108
-------
£1:37:2497/05/19
LASCO TUBES
- 1.896
5.245
t.237
HIGH
ro
ro
6
NO
s
4.813
7.662
10. i
CHROHftTOGRAn 1 P1EI10RIZED
CR581 CHROMATOPAC
CHAHHEL HO 1
SAMPLE MO 8
REPORT MO £41
PKMO
1
2
3
4
5
6
7
8
9
10
11
IE
13
14
15
16
TIME
AREA UK IDM0
FILE
METHOD
COMC
G
0002
MAHE
1.896
3.02
3.727
4.013
5.245
6.237
6.9
7.662
8.955
9.275
9.482
9.626
16.169
10.408
10.506
10.824
84 10
1812
406
£31512
16462
352
1925615
457
5929
463
5570
3153635
3301385
1219
1823
3980
V
VE
VE
y
V
V
2.6882 CS2
£2.3593 MMA
1
2
36.6185 STYREME
33.3341 CUMEME
TOTAL
8652968
100
-------
i:l :58: 3297/05/19
LASCO TUBES
— 1.894
5.246
6.239
HKti
4.613
7.664
-* -u'
r tun
CHROMATOGRAM 1 MEMORIZED
CR581 CHROtlATOPAC
CHANNEL MO 1
SAMPLE HO 9
REPORT HO 242
i-. 112
FILE
METHOD
G
0902
PKHO
TIME
AREA !1K I DUO
CONC
MA ME
I
£
o
*r
4
5
6
7
3
9
IB
11
12
13
14
15
1.894
3.868
3.725
4.913
5.246
6.239
6.903
7.664
9.282
9.631
9.891
10.112
19.508
10.704
18.824
7373
1733
395
227633
10147
338
1874940
399
2003
3104427
3953
3221358
422
• 2651
122Q
VE
V
SVE
T
TV
TV
TOTAL
8458593
£.7008 CS2
22.2456 MMA
16.8331 STYREME
38.2205 CUMEME
KJ
CJ
6
3
1GG
-------
££: 19:£597/95/19
LASCO TUBES
tLK
1.898
3.8S3
=^=-
5. £45
6. £3 6
8.74
4.811
;HROHftTOGRAH
MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKHO
1
£
3
4
5
6
7
8
9
10
CHROI1ATOPAC
HO 1
HO 9
HO £43
TIME
• 1.898
3.9S3
4.811
5.245
6.236
8.74
9.283
9.716
18.392
10.792
fiREA MK
1431
779
212487
\3927
286
5352
4489
4118 V
1473
3766 V
ID HO
4
1
FILE
METHOD
CQNC
0
9802
HA HE
98.G988 CSS
1.9012 STYRENE
-------
TOTAL £36107
£2:40:1497/95/19
100
LASCO TUBES
1.896
3.021
5.247
6.237
>3
i3
4.Q13
CHROI1ATOGRAM 1 MEMORIZED
CR591 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO O
REPORT HO 244
o
en
:'KNO
TIME
AREA UK IDNO
FILE
METHOD
CONC
O
OBOE-
1
2
3
4
5
6
7
8
1.396
3.021
4.013
5.247
6.237
9.733
18.11
10.563
1723
941
238532
4818
349
4315
3869
3848
KJ
to
u>
6
ro
O
OO
VI
6
NJ
1
2
96.633 CSc
1.7488 STYRENE
1.5681 CUMEME
TOTAL
258395
100
-------
3:81:8397/85/19
1.58
3.086
, 4,005
• 5. £4
6. £31
I ii.fb""-
1 10.777
CHRQMATOGRAM 1
CR581 CHROPIATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT HO £45
F'KMO TIME
1 1.58
£ 3.886
3 4.805
4 5. £4
5 6. £31
6 6.895
7 9.467
8 9.6££
9 10.186
10 10. £16
11
18.777
TOTAL
,-! i .-- "i
MEMORIZED
AREA UK
683
,A-*568E
385378
3399
278
43376
348£
£9£067 V
1887
711 V
4446
568588
LASCO TUBES-
FILE 8
METHOD 0082
I DM0 COHC NAME
4 37.3485 CSS *
3 7.9939 MMA
1 53.8262 STYREH
2 8. £883 CUMEME
£ 0.1311 CUMEME
108
ftF-S-T.
-------
...c'l:5397/05/19
1.58
• 3.8Q7
, 4.888
• 5. £45
6.236
f 10,1 Bo" ' *
* 10.83
CHROMATOGRAtl 1
CR501 CHROMATOPAC
CHANNEL MO 1
SAMPLE HO 9
REPORT NO £46
PKHQ TIME
1 1.58
£ .- 3.887
3 4.888
4 5. £45
5 6.236
6 6.3
7 9.5
8 9.6E7
'3 18.186
18 10.83 '
ET
'
MEMORIZED
AREA . MK
688
5703
208517
3461
285
4483E
£26 V
3851 7£ V
375
4784
LASCO TUBES
FILE 8
METHOD 888£
IBNO COHC NAME
4 37.3887 C32
3 8.8215 MMA
1 54.6986 STVRENE
2 8.8672 CUMEME
AF'5-1
FH
K]
KJ
1*1
6
8
u
•si
6
-------
TOTfiL 574043
3:42:4397/05/1 9
4.Gil
1.398
3.888
===-
5.247
6. £37
Ci £ £ O
8-.I&2
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHAMMEL HO 1
SAMPLE HO 8
REPORT HO £47
PKHO
TIME
AREA IIK IDM0
• 108
LASCO TUBES
BN
FILE
METHOD
COMC
0
0082
HA ME
1
£
3
4
5
6
7
. 1.
'•3'.
4.
5.
6.
9.
18.
898
08.8-
811
247
237
663
882
692
685
286985
3754
273
3892
3821 V
4
1
2
96
1
1
.7671
.8282
.4127
TOTAL
21922S
100
-------
36:03:2697/05/20
1.399
3.608
, 4.608
5. £43
6. £34
18.174
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 248
PKHO TIME AREA MK
1 1.899 67£
£ 3.Q88 631
3 4.008 208826
4 5. £43 381G
5 6.234 279
6 10.174 1613
LASCO TUBES
FILE 9
METHOD 0082
I DM0 CONC KiPfHE
4 99.2333 CS2
2 0.7667 CUHEM
ftf-s-z
a
01
CJ
6
8
U)
TOTAL
215881
100
-------
CHROMAT
i0:£4:0697/f
1:!§8
3.987
' —
• 5. £4
6.. £31
1 Q.892"-'"
OGRAM 1
CR5G1 CHROMATOPAC
CHANNEL MO 1
SAMPLE NO 8
REPORT NO £49
PKMQ TIME
1 -,. 1.58
£ 1.898
3 3.007^
4 4.006'*
.5 5.24
6 6.231
7 6.895
8 9.62
9 18.892
J5/28
4.886
MEMORIZED
AREA MK
680
334
4992 ••
£0438£
3576
£74
39937
514847
645
LASCO TUBES * ^
1*1-
/ —
/] r"
/ 1 ^^
FILE O
METHOD 800£
I UNO CONC NAME
4 £6.899 CS2
3 5.2562 MMA
1 67.7599 STYREHE
£ 8.8849 CUMEME
•-5-Z .
Ft/fr/ft)^
I
TOTAL
769667
100
-------
hi82
3.009
•••••I
5.£4
6. £3
-t_894
LASCO TUBES
4.80?
o
03
CHRQMATQGRAM 1 MEMORIZED
CR591 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO 6
REPORT NO 250
PKHO
TI'HE
AREA UK IDHO
1 •
2
3
4
5
6
?
8
9
10
11
12
1.582
1.9
3.009
4.00?
5.24
6.23
6.894
9.358
9.619
9.758
18.099
10.4
687
338
5839
£05812
3608
276
4837?
2Q86
512703
3118
848
1169
FILE
HETHOD
COHC
0
0882
NAME
o
U)
27.6898 CS2
5.3146 MMA
67.484 STYREHE
0.1116 CUMEME
-------
TOTAL 775982
Di:05:1797/05/29
1.895
3.015
—
5. £37
6. ££3
4.903
CHROHATOGRAtl 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO G
REPORT NO £51
LASCQ TUBES
AF3-5- 2.
PKNO
1
^•,
c
3
4
5
TIHE
1.395
3.015
4.ti03
5. £37
6. ££3
AREA
1093
705
£13951
4Q64
£94
IDHO
FILE
METHOD
CONC
100
0
0002
MANE
-oc.
-------
TOTAL 225107
01:£5:5597/95/29
1.893
3
5.233
6.224
100
LASCO TUBES
i.999
CHROflATOGRAfl 1 MEMORIZED
CR501 CHROflATOPAC
CHAHNEL HO 1
SAMPLE MO 0
REPORT NO 252
PKNQ
TIME
AREA f1K IDMO
1
^t
c
3
4
5
1.893
3
3.999
5.233
6.224
1024
655
286906
374G
269
FILE
METHOD
CONC
100
0
8002
NAME
C52
U)
6
8
u
VI
6
fO
-------
TOTAL £12595
100
Jl :46:3197/
ir n i
:|i|
L. • I T I
3.Q16
==—
• 5. £57
6. ££9
V- 6.S93
8.795
1 111 it*
CHROMATOGRAM 1
CR5Q1
CHANNEL
SAMPLE
REPORT
PKNO
1
c
3
4
5
6
i'
8
9
IB
11
12
13
CHROMATOPAC
, HO 1
HO 0
HO £53
T I ME
1.581
1.895
-VS. 141
3.016
4.004
5. £37
b.2£9
6.893
8.795
9.618
10.095
10.411
10.66
95/20
4.004
MEMORIZED
AREA UK
£006
783
495 V
1£00
£84501
3487
349
11724
12644
426375
3765 V
. 910
7296 V
LASCO TUBES (V
ft
FILE 0
METHOD 0002
IDNO CONC NAME
4 31.6387 CS2
3 1.8133 MHfl
1 65.9649 STYREHE
£ 0.58£6 CUMEME
-------
TOTAL 675534
J2507S8897/85/28
188
LASCO TUBES
fH A
3.8Q8
===^m
£41
£31
I— 6.897
4,887
o
->a
o
CHROMATOGRAtl 1 MEMORIZED
CR581 CHR011ATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT HO £54
PKNO
i
£
3
4
5
6
7
8
9
18
11
12
TIME
1.531
1.895
8.141
3.808
0S7
,241
,231
,897
,381
,622
18.892
18.416
AREA UK IDHO
FILE
METHOD
COHC
0
008E
NAME
to
NJ
U)
6
ro
4.
5.
6,
6,
9,
9.
2869
888
498
1203
885281
3501
375
11888
1672
431523
2456
677
y
V
V
1
2
31.526 CS2
1.8257 tit!A
66.£711 STYRENE
8.3772 CUMEME
-------
32:£7:3297/95/28
1.896
5. £35
b.££6
LASCO 1UBLS
I/'
BH
CHROI1ATOGRAI1 1 MEMORIZED
CR5B1 CHROIIflTOPflC
.CHANNEL NO 1
SAMPLE HO Q
REPORT NO £55
PKNO
TIME
AREA UK IDNO
FILE
METHOD
CONC
0
0802
NAME
1
c
o
4
5
1.396
3
. 4
^;;5.£35
."•'.6.226
579
708
£19353
';• 3963
£96
190
CS2
-------
TOTAL 224899
2:48:6197/55/29
1.897
3.068
5.233
6.233
\ 10.48
4.008
109
LASCO TUBES
\0-5-2.
BH
CHROMATOGRAtl 1 I1EMORIZEB
CR501 CHROtlATOPAC
CHANNEL NO 1
SAMPLE NO 9
REPORT HO 256
PKNO
TItlE
AREA MK IDNO
1
2
3
4
5
6
1.897
3.008
4.008
5.233
6.233
10.48
589
654
207029
3679
273
5399
FILE
METHOD
CONC
109
9
8002
N]
N]
CJ
6
8
MAME
CS2
-------
TOTAL 217544
33:08:3297/05/20
10B
LASCQ
TUBES
3.OD4
5.£25
6.223
-tr.888
FH A
3.999
CHROMATQGRAH 1 MEMORIZED
CR5Q1 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO £57
PKNO
1
£
3
4
5
6
7
, o,
3,
TIME
004
999
5.225
6.223
6.888
9.614
10.099
AREA UK IDNO
4180
£06646 4
FILE
METHOD
CONG
0
0002
NAME
°129
o
279
31430
£32442
1412
£
43.7S73 CS2
6.6599 NMA
49.2535 STYREHE
0.2993 CUMEI1E
-------
IUIAL
13:£9:0£97/85/£a
186
LftSCO TUBES
fti l\
4.QQ6
5.24
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMfiTQPAC
CHANNEL NO 1
SAMPLE HO 9
REPORT HO £58
PKNO
1
'£
3
4
5
6
7
TIME AREA UK IDNO
4145
£05681 4
3063
£73
3Q7Q2 3
££7643 1
18.892 468 £
3
4,
5,
6.
6,
9,
066
£4
£3
895
62
FILE
METHOD
COHC
0
9902
HAME
44.£886
6.6183 MMA
49.Q7££ STYREME
8.10Q9 CUMEME
to
(*>
6
NJ
o
6
N9
-------
TOTAL 471374
33:49:3497/95/20
189
LASCG TUBES
1.899
3.Q16
Rtr'S-1
8H
4.0G3
5. £36
6.226
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 9
REPORT HO £59
PKNO
1
£
3
4
5
6
7
8
"t'-y
>•/;-:.
TIME
S99
3.816
1
4.
,5.
6,
9,
10,
993
£36
226
814
167
18.461
AREA MK
321
625
295525
3599
£63
6623
3475 V
3905 V
IDNO
4
2
FILE
METHOD
COMC
B
0992
HA ME
98.3373 CS2
1.6627 CUHEHE
-------
TOTAL ££4336
D4:89:5797/95/20
190
LASCO TUBES
1.S96
3. 814
5.£39
6. ££9
4.094
CHROHftTOGRflll 1 HEtlORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO £69
PKMO
£
3
4
5
TIME
1.896
3,014
4.004
5.239
6.229
AREA UK IDHO
321
644
['08911 4
3678
271
FILE
METHOD
COHC
100
0
G002
MfltlE
C52
KJ
N>
OJ
6
-------
TOTAL 213825
34:30:1997/95/28
1.888
3
•5.23
6.221
190
LASCO TUBES-
CHROMATOGRAH 1 MEMORIZED
CR5B1 CHROHATOPAC
CHANNEL HO 1
SAHPLE HO 0
REPORT HO 261
PKNO
TItlE
AREA flK I DUO
fe.iv
2
3
4
5
1.383
3
4
5.23
6.221
4903
1181
211266
6568
277
FILE
METHOD
CONC
190
G002
HAtlE
ess
-------
TOTAL 224194
J4:50:3197/Q5/20
190
LftSCO TUBES
1.887
3. OD8
—
5.231
6.223
i.999
CHRQttATQGRAtt 1 MEMORIZED
CR5G1 CHROMATOPAC
CHANNEL MO 1
SAMPLE NO 8
REPORT NO 262
FILE
flETHOD
900°
L'C
KNO
1
£
3
4
5
TIME
1.887
s.eee
3.999
5. £31
6.223
TOTAL
AREA
4788
1168
289802
6498
275
222531
MK I UNO
C 0 N C
1Q0
108
NAME
C32
10
K)
U)
s
VI
6
10
-------
LASCO TUBES
co-A/Cy? L
1.905
3.028
•
5.252
6.244
4.819
IQilDD
CHROMATOGRAM 1 MEMORIZED
o
;5
CR561 CHROHATOPAC
CHAMHEL NO 1
SAMPLE HO 8
REPORT NO £4
:IKNO
3
4
5
6
7
8
9
10
1,
3,
4
5
6
6
9
10
10
TIME
90S
028
019
£52
,244
,907
,639
,123
,533
AREA MK IDNO
1587
997
218350 4
4802
299
757277 3
FILE
METHOD
COHC
B
00G2
MAME
10.839
1749622
1607211
159
1152
SV
T
1
£
s
u>
6
N>
O
OJ
VI
6
KJ
5.Q399 CSS
17.4791 HHA
40.334 STYREHE
37.997 CUMEI1E
TOTAL
4341456
100
-------
i- || WWW
.1.981
3.024
SJ
5.248
6.239
4.Q15
IQillP
CHROMATOGRAM .1 flEMORIZEL
CR5D1 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT HO
25
PKHO
c
J
b
7
8
9
10
TIME
AREA MK IDHO
FILE
METHOD
CONC
0
9002
MAME
1.991
3.024
4.015
5.248
6.239
6.903
9.635
19.119
19.533
10.325
1615
1043
£22699
4966
332
787351
1829856
167541P
161
1261
SV
T
TOTAL
4515641
4.9419 CSS
17.4721 MMA
40.4667 STYRENE
37.1792 CUHEHE
100
-------
18:43:2497/95/21
1.587
3.016
LASCO TUBES
4,815
5.248
6.242
NJ
O
CJ
•si
6
N>
CHROMATOGRAM 1 MEMORIZED
CR561 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT NO 26
FILE
METHOD
0
B802
PKNO
1
2
3
4
5
6
7
TIME AREA f1K IDNO
.587 636
L016 4854
L015 213491 4
£42 3564
.242 232
,907 41161 3
9.636 535767 1
COMC
O C Q 7 1 C'
C O . ^ .' I C
5.2
67.678
NAME
C O
-J u
MMA
STYRENE
3
9
18.IS
18.27
1194
2614
0.1588 CUMEME
-------
TOTAL 893582
108
l7»OfiC'77f/
1.585
" 3.012
• 5.244
6.236
I IS: Iff"'
CHRONATOGRAM 1
03/ci LHbL-U lUbtis
4 fl1 1
^ * 13 I 4
MEMORIZED
-/-Z
CR501 CHROriATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO 27
FILE
METHOB
i
8002
PKNO
TIME
AREA MK IDHO
CONC
NAME
1
2
3
4
5
6
^
8
9
10
11
1.585
812
811
3.
4.
5.
6.
6.
9.
9.
10.
10.
t'44
236
9
442
628
114
,25
18.5S1
648
4846
212982
3541
233
48733
957
536639
2787
2217
2369
V
y
V
V
1
o
£ ~?-?ri< i--c^
b til O 1 l/O
5.1213 MMA
67.4713 STYREHE
0.3585 CUMEHE
0.2787 CUHEME
n.k
-------
9:£4:5397/85/21
LA8CO TUBES
- 3.8Q?
5.£41
6.232
^896
K)
W
6
8
4.809
18.18V
CHROHATOGRAH 1
CR581 CHROHATOPAC
CHANNEL MO 1
SAMPLE HO 9
REPORT HO 28
PKNO TIME
MEMORIZED
1
2
3.86?
4.Q89
AREA !1K IDHO
9618
FILE
METHOD
COMC
HAilE
48.9983 CS2
3
4
5
6
7
8
5.241
6. £32
6.896
9.45
f .624
10.108
3564
308
36285
1Q91
298765
1188
1
2
6.5224 MHA
52.2657 STYRENE
0.2136 CUHEHE
-------
IUIHL
9:45:2597/95/21
160
LASCO TUBES
MA
- 3.Q96
5.246
6.236
-fr-,981
4.011
10:09"*
CHROMATOGRAH 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE MO 8
REPORT HO 29
>KNO
TIME
AREA MK IDHO
FILE
METHOD
COMC
O
0002
MAME
1
2
i
•^
4
5
6
7
3.806
4.Q11
5.246
6.236
6.901
9.628
10.098
8833
216399
3290
£86
3353S
£71797
991
3
1
2
41.3963 CSS
'6.416 MMft
51.9961 STYREME
0.1396 CUHEME
-------
TOTAL 535133
6: 65:5497/95/21
100
LASCO TUBES
10 ~
FH-f\
I.023
5.24
6.23
6.895
K)
10
CO
6
K)
o
OJ
4.697
18:1?$
CHROHATOGRAtl 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL MO 1
SAMPLE HO 0
REPORT MO 3G
FILE
METHOD
0
0002
PKNO
TIME
AREA II K I DUO
COHC
NAME
1
2
1.367
1.581
219
1546
3
4
5
6
7
3
9
10
11
12
13
14
2,
r,
O
4
5
6
6
9
9
9
19
875
141
007
,24
,23
,895
,267
,375
,621
,Q92
10.419
546
529
726
213140
2836
. 388
7050
415
2196
372292
619
327
V
V
3
1
2
35.9365 CS2
1.1386 HHA
62.7705 STYREME
Q.1Q44 CUMEME
-------
TOTAL 662829
..•8:26:2197/05/21
180
LASCO TUBES
\o-l-]
i. £63
I • 9 t1 U
v • v p 0
L. • I C J
3.Q2
5. £41
6.£31
6.893
4.096
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL MO 1
SAMPLE MO D
REPORT MO 31
FILE
METHOD
0
OQG2
>KNO
TIME
AREA MK I UNO
CONC
NAME
1
£
3
4
5
6
7
8
9
10
11
12
13
1.367
1.577
1.S83
£.125
3
4
5
6
6
9
9
10
92
066
241
£31
398
,367
,6£4
,104
10.419
£21
1547
539
5£7
741
£13633
2818
380
6951
252
365549
524
301
36.4153 CSE
1.1849 MMA
62.3106 STYREHE
0.8393 CUMEME
OJ
6
KO
s
V4
6
to
-------
,:fl! 46:4697/95/81
LASCQ TUBES
!:«?
=5
5. £37
6. £17
-9.621
fHA
4.004
CHROMATOGRAH 1 MEttORlZEI)
CR5Q1 CHROtlATOPAC
CHANNEL NO 1
SAMPLE MO 8
REPORT HO 32
FILE
METHOD
0
0002
PKMO
1
2
3
4
5
8
3
10
TIME'
1.33
1.58
1.875
£.139
3.823
3.437
4.Q04
5. £37
6.217
9.621
AREA MK IDM0
916
6575
1922
1924 V
1663
790
224232 4
3821
572
£4514 1
COMC
NAME
9Q.1451 CS2
9.8549 STYREME
-------
TOTAL
:669£8
Ji:G7:0£97/05/£l
10Q
LASCO TUBES
9-f-Z
5.£33
6. £22
-9.617
CHKOtlATOGRAH
1 MEMORIZED
CO
CR5B1 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO O
REPORT HO 33
PKMO TIME AREA MK IBNO
1 1.379 961
£ 1.578 6435
3 1.882 1868
4 £.137 186£ V
5 3.8£1 1611
6 3.425 755
7 4 £170£7 4
8 5.£33 36£8
9 6.222 546
10 9.617 22890 1
FILE
METHOD
COHC
0
i380£
NAME
to
ro
CO
6
vj
6
KO
99.459 -CS£
9.541 STYREHE
-------
hll!
3.8Q4
5. ££5
6.889
FHfl
[19.095
CHROMATOGRAI1 1
CR5B1 CHRQHATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO 34
MEMORIZED
PKMO
TIME
AREA UK IDNO
FILE
METHOD
CONC
8
QBB2
NAME
1
2
3
4
5
6
•^
f
8
1.567
1.891
,. 3.Q94
4
5.2£5
6.889
9.613
10.995
234
896
2514
£17622
1858-
743
477292
1859
31.2354 CS2
8.1866 HMA
68.506 .STYREHE
8.152 CUI1EHE
-------
TOTflL 78221B
,_'l:4?;2997/85/2i
188
LASCO TUBES
i.884
, , am
5.225
6.883
3.999
18.999
CHROMATOGRAI1
1 I1EMORI2ED
CR501 CHROnATQPAC
CHftNHEL HO 1
SAMPLE NO Q
REPORT NO 35
PKNO
TIME
AREA UK IDNO
FILE
METHOD
COHC
o
10
NAME
i
2
3
4
5
6
7
B
1.578
1.894
3.804
3.999
5. £25
6.883
9.617
18.099
228
837
2364
£11048
1737
694
448881
982
NJ
ro
31.9633 CSS
0.1849 MMA
67.8435 STYRENE
Q.1484 CUMEME
-------
1.567
3.Q84
5.£31
6,££2
6.891
3.998
18.098
CHROHATOGRfttl 1 MEMORIZED
CR5B1 CHROttATOPAC
CHANNEL NO 1
SAMPLE NO 9
REPORT NO 36
FILE
METHOD
8
0002
PKMO
TH1E
AREA [1K I UNO
COHC
NAME
1
2
3
4
5
6
7
8
1.567
3.BQ4
3,998
5.231
6.222
6.891
9.616
19.098
284
1703
217452
3283
401
408
428194
1S66
33.6931
CS2
3
0.0631 tltt A
66.1692 STYREHE
8.1647 CUttEHE
-------
TOTAL 65E71E
££: £7'.5897/95/21
1S0
LASCO TUBES
Fit
3.QB6
5.£32
6.222
6. 883
7.934
3.999
1.8.099
CHROtlATOGRAfl 1 I1EHORIZED
CR581
CHANNEL
SAMPLE
REPORT
FKNO
1
£
3
4
5
6
7
8
CHROI1ATOPAC
HO 1
•HO B
HO 37
TIME
3.986
3.999
5.23£
6.222
6.883
7.934
9.617
10.099
AREA MK IDHO
1671
£15931 4
3232
397
411 3
£55 -
421774 1
1051 £
FILE
METHOD
COHC
0
9002
HA HE
*-i *"i •? n *•• •-» r- r-
O i . f O O C L- O
0.8642 Mttft
65.9882 STYREHE
9.1644 CUHEHE
UJ
6
ro
O
UJ
VI
6
-------
LASCO TUBES
-.T- /
\m
.3.912
===i
5.231.
6.221
CHROI1ATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHAHMEL NO 1
SAMPLE MO 0
REPORT NO 38
PKHO
1
H
3
6
7
TIME AREA UK 1DHO
1.367 163
577 808
,896 465
,Q12 4£8
222423 4
,231 3842
6.221 289
F.ILE
METHOD
CONC
NAME
1.
1,
3.
4
5,
1GG
CS2
-------
TOTAL 228418
CHROMAT
jiwotiecV'M
1O Jt f
:H5
3.013
5. ££5
b.££4
OGRAM 1
CR5G1 CHROMATOPAC
CHANNEL HO 1
SAMPLE MO 8
REPORT HO 39
PKHO TIME
1 1.576
2 ' 1.895
3 3.013
4 4.002
5 5.225
6 6. £24
33/C 1
• 4.002
MEMORIZED
AREA M
784
453
406
£15156
3638
£7£
108
LASCO TUBES
fHA
IDM0
FILE
METHOD
COMC
8
0802
HA ME
106
CSS
fs)
KO
CO
-------
TOTAL £28708
'3:£8:1497/65/£l
3.Q99
==^— 3.997
5. ££9
6.££
7.931
CHROI1ATOGRAM 1 MEMORIZED
180
LASCO TUBES
FHA
CR501 CHROI1ATOPAC
CHANNEL HO 1
SAMPLE NO 3
REPORT NO ,.4.0
TILE .
METHOD
0
000£
PKMO
1
£
3
4
5
TIME
3.099
3.997
5.£29
&.££
7.931
=: AREA HK IDNO CQNC
484
£16786 4 100
3469
388
39G
HAME
CS£
-------
221517
£3:48:1397/95/21
1.088
5.228
6. £08
7.917
1.996
CHROMATOGRAM 1 MEMORIZED
CR5G1 CHROMATOPAC
190
LASCO TUBES
SAMPLE
REPORT
PKMQ
1
'•i
L.
3
4
5
L. I1U 1
HO 0
HO 41
TIME
3.008
3.996
5.228
6. £08
7.917
FILE
METHOD
AREA MK IDHO
467
£14443 4
3397
386
388
COMC
100
-f-Z
NAME
CS2
10
K>
CJ
-------
TOTAL 2190
30:08:1397/05/2
3 . 6 1 £
===>^— 3.
5.231
6.219
ft -•• fi ~!
80
2 LASC
999
189
TUBES
o
8
6
to
CHROMATOGRAM 1 MEMORIZED
CR5G1 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO 3
REPORT NO 42
FILE
METHOD
9
9002
PKMO
1
2
3
4
5
6
7
TIME
3.012
3.999
231
219
AREA UK IDM0' COMC
NAME
5.
6,
6,
9,
883
687
10.036
379
219146 4
3384
393
93793 3
196351 1
247201 2
28.9688 CS2
12.3984 MMA
£5.9555 STYREHE
32.6773 CUMEME
-------
3.067
• ' —
5. £28
6.288
3.996
CHROHATOGRAM 1 MEMORIZED
CR5Q1
CHANNEL
SAMPLE
REPORT
PKMO
1
c
3
4
5
6
CHROMATOPAC
MO 1
HO 8
NO 43
TIME
3.067
3.996
5. ££8
6. £88
6.832
9.611
10.092
AREA t1K IDNQ
3/9
220439 4
3424
395
95879 3
199217 1
250869 £
FILE
METHOD
COMC
0
8882
NAME
£8.7931 CSS
12.4173 MMA
26.BE1E STYREHE
32.7679 CUMEME
-------
TOTAL 769785
18:48:0397/85/22
LASCO TUBES
3. 987
j
5.23
6.288
6
IO
3.998
SiQOO
CHROMATOGRA11 1 MEMORIZED
CR5B1 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO G
REPORT HO 44
PKNO
TIME
AREA UK I UNO
FILE
METHOD
COMC
0
0882
NAME
1
2
3
4
5
7
3.8Q7
3.998
5.23
6. £88
6.833
9.612
18.893
378
£23764
3483
468
552721
1853672
1288188
1
2
7.3843 CS2
18.2481 UNA
34.7717 STYRENE
39.6639 CUMEME
-------
11:97:5297/85/22
i.005
5. ££7
6.£08
LASCO TUBES
u i 001
I 10.8Q4
CHROHATQGRAH 1
MEMORIZED
CR5B1 CHROHATOPflC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO 45
FILE
METHOD
9
8892
PKHO
TIME
AREA IIK I UNO
COHC
NAME
3
4
5
6
7
8
3.
005
995
5.227
6.£08
6.881
9.61
10.09
10.804
369
££0497
3386
458
538699
182786Q
1173132
385
7.4467 GS2.
18. 1981 MMft
34.7228 STYRENE
39.6303 CUMEME
-------
TOTflL 2964786
:ii:£7:4197/95/££
100
LASCQ TUBES
6
ro
O
6
IS)
3.996
6.£16
OiOOl
9. £64
CHROHATOGRAI1 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE NO 0
REPORT HO 46
PKHO
TItlE
AREA UK IDM0
FILE
METHOD
CONC
000S
NAME
1
£
3
4
5
6
7
8
3.996
6. £16
6.881
9. £64
9.61
10.09
10.483
19.S85
£15931
1161
111714Q
£69
£184049
£313958
336
68£
3./S46 C3£
19.4£49 MMfl
36.5353 STYREME
4Q.£35£ CUHEME
-------
6.£11
3.989
OiD
q.gfeg
CHROMATOGRAH 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL MO 1
SAMPLE MO 8
REPORT NO 47
PKMO
1
£
3
4
5
6
7
3
TIME
AREA f1K IDNO
FILE
METHOD
COMC
0
8082
NAME
3.989
6. £11
6.876
9J""1 iL O
• CDC
9.688
18.889
10.487
18.884
£22711
1££3
1175894
£73
£283797
£4£8783
359
685
TOTAL
3.6981 C32
19.51£4 MMft
36.5925 3TYRENE
49.197 CUHEHE
100
K>
K>
-------
J2:07:0497/05/22
1.885
2.992
^=^==
5.224
6.214
LflSCO TUBES
CJ
CO
•vj
6
NJ
CHROHATOGRAtl 1 HEHORIZED
CR501 CHROMATOPAC
CHANNEL MO 1
SAHPLE MO 8
REPORT NO 48
FILE
METHOD
0
G002
FKMO
1
2
3
4
5
6
7
8
9
10
11
TIHE
*:.. ARE ft UK ID NO
CONC
NAME
1.885
2.992
3.991
5.224
6.214
6.879
9.608
10.087
10.408
10.5
10.798
1392
951
217162
4512
282
713704
1650673
1514010
630
298
1111
5.3824 CSS
17.4E63 flMft
40.3841 STYREHE
36.9672 CUNEME
TOTAL
4104723
100
-------
i£:£6:3997/95/23
LASCO TUBES
1.882
£.998
=
5. ££3
6.214
i.992
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT HO 49
FKNO
TIME
AREA MK IDNO
FILE
METHOD
CONC
9
088£
NAME
1
I",
c.
3
4
5
6
7
8
9
IB
11
1.332
2.998
3.992
5.223
6.214
6.878
9.608
10.088
10.399
10.5
10.792
1397
971
222473
4725
301
754327
1760397
1615963
534
343
1205
1
j-i
5.1106 CS2
17.3283 I1MA
40.4395 STYRENE
37.1216 CUMEME
CO
CO
OJ
I
00
TOTAL
4362684
100
-------
1.904
3.817
5.£52
6.245
4.818
e
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT HO 36
PKMO
TIME
AREA MK IDHO
FILE
METHOD
COHC
0
00-02
HAME
1
•-,
3
4
5
6
7
3
q
10
11
1.904
3.017
4.818
5.252
" 6.245
b.908
9.64
10.123
10.45
10.526
10.841
1086
972
214516
4684
301
762476
1813355
1667710
1020
376
1161
4.8119 CS2
17.1033 MMA
40.6759 STYRENE
37.4089 CUMEME
TOTAL
4467656
1 FiPi
-------
TOTAL 18789
6:13:5597/05/22
1.903
3.025
109
LASCO TUBES
4.815
5.248
6.241
I ii:§f3
CHROI1ATOGRAH 1
CR5B1 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO G
REPORT HO 35
MEMORIZED
PKNO
TIME
AREA UK IDHO
1
2
3
4
5
6
7
8
9
10
1.903
3.025
4.015
5. £48
6.241
6.904
9.638
1Q.122
10.425
10.533
1099
961
214805
4576
299
746430
1781913
1641625
758
447
FILE
METHOD
COHC
8
GOQ2
NAME
4.8989 C32
17.8232 MMA
49.6387 STYRENE
37.439S CUMEtlE
11
10.84
TOTAL
1132
4394042
199
-------
5:5£:££97/85/££
LflSCO TUBES
NDfi -f~
4.817
5.£54
6.£42
r-
636
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHAMMEL HO 1
SAMPLE MO 0
REPORT HO. 33
FILE
METHOD
0
0902
PKNO
TIME
AREA MK IBNO
CONG
NAME
1
2
3
4
5
6
-.•,,.!.. 5 86
"1.984
4.017
5. £54
6.242
9.636
736
650
216649
1806
282
21603
98.9323 CS2
9.Q672 STYRENE
(O |
to!
-------
LflSCO TUBES
1c n c
:«92
3.031
(\
4.023
5.£57
6. £44
9-. 634
CHROMATOGRAH 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 31
OJ
6
8
OJ
XI
6
PKHO
1
il
3
4
5
6
7
TIME
1.585
1.902
3.031
4.023
5.257
6.244
9.634
AREA
866
738
329
243687
22B3
347
26914
TOTAL
FILE
METHOD
CONC
8
0002
HAHE
90.0541 CS2
9.9459 STYRENE
275133
180
-------
6. £47
6.913
tOO
19.12
CHROMATOGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHANNEL HO 1
SAMPLE
REPORT
PKNO
1
2
3
4
5
6
7
8
9
NO i
NO 29
TIME
1.983
3.819
4.823
5.S58
6.247
6.913
9.383
••' 9.638
10. \?
AREA UK IDNO
1317
5642
233758 4
2148
383
1254 3
327
681085 V 1
2988 V 2'
FILE
METHOD
CONG
8
0082
NAME
25.4611 CS2
Q.1366 MHA
74.1757 STYREHE
8.2266 CUMEHE
-------
TOTAL £££001
4:47:5497/85/22
10B
LflSCO TUBES
1.9
3.017
5. £57
6. £47
6.913
fU
4.022
MEMORIZED
10.119
CHROMAT.OGRAM 1
CR561 CHROMATOPAC
CHANNEL MO 1
SAMPLE MO 0
REPORT MO 27
PKNO TIME AREA UK I HMO
1 . 1.9 1325
2 3.017 5705
3 4.022 238302 4
4 5.257 2165
5 6.247 310
6 6.913 1275 3
7 9.333 300
8 9.638 688527 1
'? 10.119 1377 2
FILE
METHOD
COHC
0
S002
NAME
25.6382 CS2
0.1371 IIHfl
74.0765 STYRENE
9.14S2 CUMEME
-------
1.965
3.828
=—— 4.016
5.£52
6.241
3. 637
CHROHATOGRAN 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO Q
REPORT NO £6
PKHO
1
£
3
4
5
6
TIME
..995
028
016
£52
,241
9.637
AREA MK I UNO
501
482
214553 4
2014
373
4077 1
FILE
METHOD
COHC
B
QQ02
10
NAME
98.1352 CS2
1.8647 STYRENE
-------
TOTAL 235124
I -t: us: 179//F
1.892
3.017
==—
5. £55
6. £44
• 9.638
CHROtlATOGRAfl 1
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO £5
PKMO TIME
1 1.892
£ 3.017
3 4.019
4 5. £55
5 6.844
6 9.638
I5/2E
4.919
MEMORIZED
AREA
513
521
£21147
2138
4G5
4455
UK
1U0
LftSCO TUBES
9 '
r
I*
UNO
FILE
METHOD
COHC
e
0902
HA ME
98.9254 CSS
1.9746 STYRENE
-------
13:43:4797/95/22
3.031
4.008
LflSCO TUBES
5.252
6.233
9.638
CHROI1ATOGRAI1 1 HEMORIZED
CR501 CHROI1ATOPAC
CHAMMEL MO 1
SAMPLE HO 0
REPORT HO 24
PKNO
TIME
AREA UK IDNO
1
2
3
4
5
6
7
8
9
1.375
1.584
1.899
2.147
3.031
4.008
5.252
6.233
9.638
448
2065
1700
609
681
225301
2031
408
1961
FILE
METHOD
COHC
0
0002
HAI1E
99.137 CS2
9.863 STYRENE
ro
s>
u
6
ro
O
u
VI
6
IS)
-------
3.829
,
5. £48
6. £37
9.632
CHROMATQGRAtl 1
CR501 CHROHATOPAC
CHAHHEL HO 1
SAMPLE NO 9
REPORT NO £3
PKMO TIME
1 1.331
2 1.582
3 1.897
4 £.133
5 3.829
6 4.014
7 5. £48
8 6. £37
9 9.632
TOTAL
4.614
MEMORIZED
AREA MK
456
£085
1719
6 1 8 V
603
££5356
2827
411
1358
235132
IDHO
FILE
METHOD
COMC
B
GQB£
HAHE
99.1321 CS2
•8.8179 STYREHE
180
-------
3:68:3597/85/22
1.898
3.026
LflSCO TUBES
5.£53
6.£43
10-3-I
4.819
ro
CO
CHROI1ATOGRAI1 1 MEttORIZED
CR501 CHROMATOPAC
CHANNEL MO i
SAMPLE HO 8
REPORT, HO £2
PKNO
TIME
AREA MK IBNO
1
£
3
4
5
1.398
3.9.26
4.919
5. £53
6. £43
£15£
418
230879
£364
38£
TOTAL
£36115
FILE
METHOD
CONC
100
1 flfl
0
0862
NAME
CS2
10
is)
U
6
to
o
6
Is)
-------
TOTAL 583433
£:38:£697/95/££
1.898
3.0£7
5. £54
6. £33
4.8££
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO G
REPORT HO £1
180
LASCO TUBES
PKMO
TIME
AREA MK IDMO
1
£
3
4
5
1.898
3.827
4.8££
5. £54
c •:• o o
D > L. OO
£35b
454
2491£0
2667
347
TOTAL
254944
FILE
METHOD
COMC
100
100
0
GO 62
NAME
C3£
-------
CHROMAT
18:47:4797/0
5. £07
6.183
— 9.584
OGRAM 1 1
1UCI
LASCO TUBES.
976
ro
ro
6
g
6
ro
MEMORIZED
CR5B1 CHROMATOPAC
CHAMHEL NO 1
SAMPLE NO 8
REPORT NO 56
PKHQ
TIME
AREA MK IDHO
FILE
METHOD
CQNC
9
eeee
HA ME
1
£
3
4
5
6
7
8
9
10
1.365
1.564
1.871
£.108
2.938
3.488
3.976
5. £07
6. 183
9.584
398
5£8£
1878
1330
1818
418
£19716
£007
386
13869
TOTAL
£475££
94.96S6 CS£
5.9374 STYREME
109
-------
LASCO TUBES
9-3-2.
3.96?
5.£05
6. 19
9.579
CHROMATGGRAM 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
£
o
4 *
5
6
7
8
9
10
CHROMATOPAC
NO 1
HO 8
NO 54
TIME
1.365
1.563
1.871
; £.116
£.987
3.408
3.967
5. £05
6. 19
9.579
AREA
9Q9
5£4£
1898
1348
1839
414
222193
£031
39£
13945
FILE
METHOD
COMC
0
000£
NAME
TOTAL
£50211
100
lOO
STYRENE
-------
TOTAL £27467
38:89:3397/95/22
LASCO TUBES
-7-7
3.968
5.197
6.184
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO O
REPORT NO 53
FKNO
1
£
TII1E.
3.968
5.197
6.134
AREA MK IDHO
218684
£511
••. •» ^
C ( C
FILE
METHOD
CONC
NAME
KO
KO
LJ
6
KO
o
CJ
•si
6
10
-------
7:5Q:3397/65/22
3.966
5.196
6.183
LASCO TUBES
/VM-7-1
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAMHEL HO 1
SAMPLE NO 9
REPORT NO 52
PKNQ TIME AREA MK IDHO
1 3.966 £24575
£ 5.196 2602
3 6.183 296
FILE
METHOD
CQNC
G
0002
NAME
-------
TOTAL £56951
37:32:5197/95/22
l:g§7
£.969
109
LASCO TUBES
3.963
573
CHROMflTOGRAH 1 MEMORIZED
CR501 CHROtlfiTOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO 51
PKHO
AREA HK I HMO
FILE
METHOD
COMC
10
(O
u
6
CO
•si
6
HAI1E
1
o
1
Tj
4
5
6
•j
i
1.56
1.S67
2.969
3.963
4.805
5.183
9.573
927
£618
2166
223538
319
2220
25295
TOTAL
:56987
1QO
IQO
STYREHE
-------
J7:14:£797/85/22
l:g§5
£.965
—
5.186
6.174
LASCO TUBE
ftl ft
3.957
CHROMATQGRAM
1 MEMORIZED
CR5B1 CHROI1ATOPAC
CHflNMEL HO 1
SAMPLE HO 9
REPORT HO 59
FILE
METHOD
O
09B£
PKMQ
TIME
AREA MK IDNO
CONC
NAME
£
3
4
5
6
1.56
1.865
£.965
3.957
5.186
6. 174
9.565
9.733
917
£650
2174
££3366
££41
£75
22629
£699
V
39.3448 STYRENE
10.655E STYREME
-------
1.3S1
£.983
—
5.213
6.282
3.934
I \tirn
CHROflATOGRAtl 1 MEMORIZED
CR501 CHROHftTOPAC
CHANNEL NO 1
SAMPLE MO 8
REPORT MO 72
FILE
METHOD
0
0802
PKNO
TIME
AREA MK IDHO
COMC
MAME
1.881
TOTAL
757
u
O
4 .
C
6
7
8
q
10
11
£.983
3.984
'-• 5.213
... 6.292
6.86?
9.595
18.073
18.381
10.483
1Q.775
930
£28819
' 4628
• 384
760739
133535S'
1688369
628
366
1029
4513918
4.9814 CS2
16.8853 MMA
48.7379 STYREHE
37.4754 CUMEttE
108
ro
ro
-------
1 . 885
5. £21
6.211
6
NO
3.991
«+
CHRQt1ATOGRAI1 1 MEMORIZED
CR5G1 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 9
REPORT HO 73
FILE
METHOD
G
8902
PKNO
TIME
AREA UK IDNO
CONC
NAME
c
3
4
5
6
1.885
£.999
3.991
5.221
6.211'
6.876
720
S97
216214
437G
£95
735306
4.S917 CS£
16.6356 IIHA
7
8
9
10
9.6Q4
IB.682
19.394
10.783
TOTAL
1305627
1662881
1470
896
44£8674
40.351 STYREME
37.6215 CUMEME
108
-------
1.569
F/M
3.991
6.214
9.669
CHROMftTOGRAM 1 MEMORIZED
CR501 CHROMATOPftC
CHANNEL MO 1
Is)
10
o
ui
NJ
6
N)
FILE
V
R
p
AMPLE
EPORT
KMO
1
2
3
4
NO 0
HO 71
TIME
1.569
3.991
6.214
9.609
AREA MK
1196
2Q741?
1140
2163
t
IDHO
4
1
IETHOD
CONC
96.
1.
968
032
TOTAL
G0BS
NAME
£ 11917
STYRENE
106
-------
TOTAL 427933
D4: 46: 0.497/05/23
1.571
:.991
6.212
9.685
CHRONATOGRAM. 1 MEMORIZED
CR5B1 CHROMATOPAC
CHAHMEL MO 1
SAMPLE HO 8
REPORT HO 70
PKNO
1
3
3
4
TIME
3.991
6.212
9.685
AREA MK I UNO
1283
£03794
1105
2039
100
LASCO TUBES
FILE
METHOD
CQNC
0
9002
NAME
99.0894 C32
0.9986 STYREME
-------
TOTAL 425880
J4:£6:8497/85/23
1.569
£.985
3.988
6.21
6.881
18B
LASCO TUBES
Fttfi
OJ
6
8
•6
(O
10.
CHROMATQGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAHHEL HO 1
SAMPLE HO 8
REPORT HO 69
PKNO
1
£
3
4
5
6
7
TIME
569
985
988
21
881
605
1.
2.
3.
6.
6
9.
10.088
AREA MK I DUO
667
6809
207338 4
1143
£96 3
£11971 1
510 £
FILE
METHOD
CONC
9
6882
NAME
49.3527 CS2
0.0703 MMA
50.4556 STYRENE
8.1214 CUMEME
-------
- £.987
6. £11
6.881
CHROttATOGRAn 1 MEMORIZED
CR5B1 CHROI1ATOPAC
CHAHNEL HO 1
SAMPLE NO 8
REPORT NO 68
F'KMO
TIME
AREA UK I DUO
FILE
METHOD
COMC
8
8802
MAI1E
1
?
3
4
5
6
1.569
£.987
3.99
. 6.211
, 6. SSI
9.603
672
6048
£06845
1144
308
£10373
1Q.U31
499
49.4824 CS2
8.9713 MMA
58.32.65 STYRENE
0.1194 CUMEHE
-------
T v • u v.' y f 'C'J'CO
i.57,
£.387
S5ZSZZSSS9BII
5.££8
6.£11
£'
A
3.991
to
N)
OJ
6
6
K)
CHROHflTOGRflH 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT NO 67
PKNO
TIME
AREA J1K IBHO
i
£
.-i
4
5
6
?
B
1.57
£.987
3.991
5. ££8
6. Ell
9<-J C Q
• O JO
9.683
18.983
399
7089
£96335
330
1143
351
683337
1928
FILE
riETHOU
;OMC
Q
000£
NAME
TOTAL
841331
£4.857 CS£
74.9113 STYREHE
Q.2318 CUMENE
IBB
-------
LASCO TUBES
-s7-/
1.569
h £.985
5.227
6.211
3.99
18.887
CHRQHATOGRfifl 1
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT NO 66
MEMORIZED
PKHO
TIME
AREA H!C I UNO
FILE
METHOD
COHC
88Q2
NAME
1
2 N •
3 ':•
4 ' ;
5
6
7
8
1.569
£.985
". 3.99
5.227
6.211
''' 9.35
9.606
10.887
402
7043
287204
338
1144
323
625243
1485
TOTAL
843173
24.8467 CS2
74.9753 STYRENE
0.1781 CUMEME
100
-------
TOTAL £15442
3:96:0597/95/23
IBB
LfiSCO TUBES
9-7-1
6. £ 16
KJ
KJ
LJ
6
KJ
o
6
K>
3.995
CHROI1ATOGRAI1 1 MEMORIZED
CR581 CHROMATOPAC
CHftHHEL HO 1
SAMPLE MO 0
REPORT NO 65
PKMO TIME AREA f1K IDHO
1 1.372 881
£ 1.571 3426
3 1.373 1146
4 2.128 1225 V
5 3.019 752
6 3.425 581
7 3.995 206266 4
8 6.216 1257
TOTAL 215454
FILE
METHOD
CONC
9
0092
HA ME
100
CS2
-------
TOTAL 855962
2:46:0597/85/23
188
LASCO TUBES
9-7-'
HIS
•u1 • T C C
•" ft H ^
b. cl c
3.991
CHROHATOGRAH 1 tlEMORIZED
CR5B1 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO 64
F'KHO
TIME
AREA MK IDNO
FILE
METHOD
CQNC
8
0062
NAME
1
£
3
4
5
6 .
7
8
1.373
.,!..- 572
1.374
2.128
3.017
3.4££
3.991
6. £12
887
3424
1146
1££9
752
502
£06253
1248
100
CS2
-------
TOTAL 372339
i£:£6:6897/65/23
109
LASCO TUBES
3.014
6.208
6.834
10- 7' Z.
3.99?
8
u>
u>
Hi in
CHROMATOGRAM 1 MEMORIZED
CR5Q1 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO Ei
REPORT MO 63 "
PKNO
1
2
3
4
5
6
7
8
q
10
11
12
13
14
1
1,
2
3
3
6
6
9
9
10
TIME
572
867
129
D14
,997
,208
,884
,365
.61
.088
10.392
10.475
19.558
10.666
AREA HK IDHO
1439
419
384
438
206092
1215
12825
718
628193
1643
538
253
1505
299
TILE
METHOD
COHC
0
B0B2
HflHE
4
3
2
24.2813 CS2
1.511 HHA
74.0136 STYREHE
0.1936 CUMEME
-------
TOTAL 731283
100
CHROMA!
CR5Q1
CHANNEL
SAMPLE
REPORT
PKNO
1
c
3
4
5
6
7
'. 8
9
10
11
12
13
i2:85:5897/f
is if?
3.808
===—
6.212
— 6.873
o •"> =;
OGRAM 1
CHROMATOPAC
HO 1
HO 0
NO 62
TIME
1.57
1.872
2.117
3.008 ,.
3.991 "'•
6.212
6.873
9.35
9.665
10.075
10.397
10.475
10.565
35/23
3.991
'. J U iJ
MEMORIZED
AREA MK
1448
425
386
447
208673
1243
13137
713
641363
189.4
523
259 V
1878 V
LASCO TUBES IV
FILE 0
METHOD 0002
ID MO COHC NAME
"•'•v . .
V,l, - ' •
4 24.1222 C32
3 1.5186 MMA
1 74. 1403 STYRENE
2 0.2189 CUMEME
-------
TOTAL 763384
Us 45:4697/95/23
100
LfiSCO TUBES
ffffl
£.993
6.214
:.991
CHRQNATOGRAH 1 MEMORIZED
CR5B1 CHROHATOPAC
CHAMHEL MO 1
SAMPLE MO 0
REPORT HO 61
(O
(O
ro
O
FILE
OETHOD
0
80GE
PKHO TIME AREA MK IDHO
1 £.993 2139
£ 3.991 £06119 . 4
3 6.214 1133
4 b.88 53320 3
5 9.35 170
6 9.6Q9 467190 1
7- 10.Q38 1221 2
CQNC
NA'ME
£8.3188 CS2
7.3£57
UNA
64.1877 STYRENE
O.1673 CUMEME
-------
£.997
6. £ 15
3.998
10.075""11"
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO D
REPORT HO 66
PKHO
TIME
AREA IIK IBNO
FILE
METHOD
COHC
9
0902
NAME
1
£
3
4 '
5
6
7
£.997
3.998
6. £15
••• 6.88
9.36£
9.607
19.875
££89
£1£784
1197
56351
£37
489359
1167
4
•I? 3
.•'•*
1
£
-•• r, ,-i < n c f- r- '•t
u O . IJ 1 U J L 0 C
7.4179 Mil A
64.418 STYREHE
9.1536 CUMEME
-------
11:05:3397/95/23
LflSCO TUBES
/*!£'/-/
•FHA
£.99
er p O 1
%.' . C -j i
6. £.15
C'. j y
1.995
18.875"""'
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
to
to
I*}
6
8
OI
6
10
FILE
METHOD
8
0002
REPORT HO 59
PKNO TIME
AREA MK IDHO
1
£
3
4
5
6
7
£.99
3.995
5. £31
6. £15
6. S3
9.607
10.875
624G
£06584
418
1143
43533
389348
127S
4
•T
o
1
2
CONC
NAME
3£.£41E CS£
6.7942 MMA
60.7651 STYREHE
0.1994 CUMEME
-------
J9: 45: £797/65/23
LftSCO TUBES
2.99
5.228
3.991
18.887
CHROMATQGRAH 1 MEMORIZED
CR5B1 CHROMATOPAC
CHAMMEL HO 1
SAMPLE HO 8
REPORT HO 58
PKMO
3
4
5
6
7
8
TIME
AREA MK IDNO
FILE
METHOD
CQNC
000£
MANE
£.99
3.991
5.223
6.212
6.873
9.35
9.605
10.887
6100
£03853
404
HIS
4£390
£07
389856
831
£
3S.4643 CS£
6.7503 MMA
68.6525 STYREHE
0.1324 CUMEME
-------
38:£5:1797/65/ei
£.93
6. £ 11
6.878
3,
CHROMATQGRAN 1 MEMORIZED
CR501 CHROMATOPAC
LASCO TUBES
ro
to
OJ
6
NJ
CHAHHEL HO 1
SAMPLE HO 0
REPORT HO 57
PKNO
TIME
TOTAL
AREA me' IDM0
FILE
HETHOD
COHC
294337
NAME
1
£
3
4
5
2.99
3.992
6. £11
6.878
9.605
6110
£06769
1138
114Q6
68914
4
3
1
72. 0££5
3.9731
£4.0044
100
-------
r £.993
6.221
6.387
3.998
FH A
CHR9MATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO Q
REPORT HO 56
PKNO
TIME
UK I DUO
FILE
METHOD
COHC
0
B902
NAME
1
2
3
4
C
2.993
3.998
6.221
*.; 6.887
'9.613
6147
£08152
1154
11634
69916
TOTAL
297994
71.8594 CS2
4.G158 MMA
£4.1333 STYRENE
199
-------
IUIRL £52476
£3:44:5197/85/22
I'BPi
•ft m V P 9
C • I C Q
190
LASCQ TUBES
5.£28
6.217
6.885
•*. 608
CHROMATOGRAM 1 MEMORIZED
CR581 CHROI1ATOPAC
CHANNEL HO 1
KJ
K)
VI
6
FILE
SAMPLE NO
REPORT HO
PKHO
1
£
3
4
5
6
7
8
9
10
11
0
55
TIME
TOTAL
AREA MK IDNO
1.371
1.571
1.874
£.128
3.014
3.417
3.996
5. ££8
6.217
6.885
9.608
715
6943
2420
£458
£012
985
208073
3724
601
1920
25525
255377
METHOD
COHC
0002
NAME
88.3467 CS2
0.8153 MMA
10.838 STYRENE
100
-------
TOTAL £15866
j23: £4: 4197/95/22
190 !
LASCO TUBES
hi!
3.999
5. £33
6. ££2
6.89
615
CHROtlATOGRAH 1 MEMORIZED
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1 '}
£
3
4
5
6
7
8
9
10
11
CHROHATOPAC
HO 1
HO 8
HO 54
TIME
1.373 «...
1.572 !
1.876
£.13
3.008
3.43
3.999
5. £33
6.222
6.89
9.615
AREA [IK IDNO
799
:V 6897
£497
£448 V
1990
994
£05825 4
3670
589
188£ 3
£5066 1
FILE
METHOD
CONC
0
8002
NAME
88.423 CSS
9.°
Q85
6t> B 0 11H ft
10.7685 STYRENE
-------
TOTAL £17537
iJ3: 84: 2997/95/22
18Q
LASCO TUBES
fH
1.999
5. £3
6.219
fa.888
9.613
CHROMATOGRAM 1 MEMORIZED
CR591 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 8
KO
KO
Ul
6
FILE
METHOD
REPORT HO 53
PKNO TIME
1
£
3
4
5
3.999
5.£3
6.319
6.888
9.613
AREA MK IBNO
2Q955£ 4
£3£1
£81
421 :•:
£499 1
CQNC
NAME
98.6297 CSS
8. 1983 (IMA
1.1719 STYRENE
-n a
-------
6.222
6.891
9.613
CHROHATOGRAM 1 MEMORIZED
CR581 CHROHATOPAC
CHANNEL NO 1
SAMPLE MO G
REPORT NO 52
PKNO
1
2
3
4
5
FILE
METHOD
8
QGB2
TIME
3.999
5. £31
b.£££
6.891
9.618
AREA
21£004
£381
£88
43£
£48£
COHC NAME
98.6444 CSS
0.2QQ8 tIHA
1.1549 STYREME
-------
CHROMATDGRAM 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
£
3
4
5
CHROMATOPAC
NO 1
HO 13
NO 51
TIME
1.573
1.89
3.992
5. £35
9.616
AREA MK IDHO
666
533
205024 4
1664
19832 1
FILE
METHOD
CONC
G
0862
NAME
91.1801 CSS
8.8199 STYREHE
ttf/
-------
- r- ;
4.GG5
5.241
-9.625
CHROMATOGRAM 1 MEMORIZED
CR561 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO 0
REPORT NO 5Q
PKNO
1
TIME
1.53
1.898
4.095
5.241
9.625
AREA MK IDNO
611
492
FILE
METHOD
CONC
0
Q002
NAME
197832
1545
13922
91.2704 CS2
3..-295 STYRENE
-------
:i:4£:£997/'B5/££
1:153
- £.998
=^=—
6. ££9
- 6.896
18. 10"6'uL
CHROI1ATGGRAM 1
CR581 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 8
REPORT HO 49
PKNO TIME
1 1.579
£ 1.894
3 • £.998
4 4.084
5 4.849
6 5.239
7 6. ££9
8 6.896
9 9.367
10 9.6£3
11 10.106
4.004
MEMORIZED
AREA 11 K
971
9£0
13S31
£01869
639
1856
£49
5304
185
337788
778
LASCO TUBES !?•£
r
h
FILE B
METHOD G00£
IDHO CONC NAME
4 , 36.99 CS2
3 8.9719 UNA
1 61.8956 STYREHE
£ 0.14£5 CUMEME
6
N)
TOTAL
563789
100
lit
-------
:i:03:4597/05/££ LASCO TUBES Pf^\2
^_ Z_j J
}:§§§
- 3.007
f
V 4.8;fe3
CHRQHAT
J , C.J
- 6.905
OGRAM 1
CR501 CHROnATOPAC
CHAMHEL HO 1
SAMPLE HO 0
REPORT HO 44
PKHO TIME
1 \.575fr.,-.
£ 1.898"'\
3 3.007
4 4.814
5 4.863
6 5.25
. 7 6.905
8 9.388
9 9.632
10 9.841
11 10.113
- -^ — -^—-
4.014
MEMORIZED
FILE ' 0
METHOD OQ02
AREA rlK I HMO CONC NAME
1079 •
-.. 1052
14642
212532 4 35.8441 CSS
728
2164
5865 3 8.9392 MMA
306
373486 V 1 62.9895 STYREHE
5686 V
1050 V 2 0. 1772 CUMEME
;
TOTAL 618592
CHROI1ATOGRAM 101 MEMORIZED
188
-------
i9:05:£197'05/£9
1.593
3.847
•; •
5.274
6.25
6.917
a A. f\ 1 .-
10. 13 ""
CHRONATOGRAH 1
CR581 . CHROtlATOPAC
CHAHHEL HO 1
SAMPLE NO 0
REPORT 10 75
:'KNO TII1E
1 1.593
2 3.047
3 4.032
4 5.274
5 6.25
6 6.917
7 9.483
3 9.649
9 10.13
4.G32
MEMORIZED
AREA HK
1518
379
£33231
500
1596
404
246
3673E0
733
LflSCO TUBES ,
/ V
FILE Q
HETHOD 6802
IDHO CONC MAtlE
4 33.76S3 CS£
3 B.667E Mtl A
1 61.0483 STYREHE
£ 9. 1217 CUMEME
K)
U
6
3
>j
6
N)
TOTAL
68592S
100
-------
8:46:0097/85/29
LftSCO TUBES
3.052
—i
5.281
6.263
4.839
o
CHRQHATQGRAtt 1 HEHORIZED
CR581 CHRQHATQPAC
CHANNEL NO 1
SAHPLE HO 9
REPORT HO 73
FILE
METHOD
9
8002
CO
K)
6
g
U)
6
N)
PKHO
TIME
AREA HK IDHO
COHC
NAttE
4
5
6
7
8
9
10
11
!£'
1.375
1.592
1.892
..-3.Q5E
4.039
5.281
6.263
9.292
9.467
9.653
19.136
1Q.454
£4£
£198
359
597
£12740
541
1566
217
976
1156430
£574
650
15.5837 CS2
34.3036 STYREHE
0.1 S76 CUHEHE
TOTAL
1379690
108
-------
8:26:5397/05/29
LftSCQ TUBES
1.849
-
5.267
6.£5
0 A 11A
:.\J
Ol
4.033
K)
S>
U)
6
N>
o
U)
V4
6
KJ
CHROnflTOGRAH 1 MEMORIZED
CR501 CHROHflTOPflC
CHANNEL HO 1
SAMPLE MO 8
REPORT HO. 71
PKMO
TII1E
TOTAL
AREA UK IDNO
1
£
3
4
5
6
7
8
9
10
11
12
1.333
1.595
1.903
2.16
3.049
4.033
5.267
6.25
9.404
9.651
10.132
10.447
258
£352
393
274
646
£28336
576
1637
977
1223044
3079
839
1454411
FILE.
METHOD
COHC
9
9002
NftME
15.E3£9 CSE
84.5542 STYRENE
0.2129 CUHEHE
100
-------
3.
n
.279
6.26
7.953
9.649
10.454
4.833
to
to
U)
6
CHRQHATQGRAH 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE NO 8
REPORT NO 69
FILE
METHOD
8
0002
PKNO
• TII1E
AREA UK I UNO
COHC
NAME
i
2
O
4
5
6
7
8
9
18
11
12
1.389
1.592
1.S98
2.157
3.055
3.466
4.033
5.279
6.26
7.958
9.649
10.454
1288
9563
2617
2664
1960
1115
236059
1135
2002
465
15616
388
93.7954 CS2
6.2846 STYRENE
TOTAL
i7479£
1GO
-------
LASCO TUBES
CHROMATOGRmi 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 68
PKHO
TIME
AREA MK I UNO
FILE
METHOD
COHC
O
0092
NAME
1
£
3
4
5
6
7
8
9
10
11
1.338
1.589
1.895
£.153
3.046
3.457
4.824
5.272
6.254.
7.958
9.65
1309
10275
2798
2841
2838
1168
242126
1172
2060
464
16883
TOTAL
282253
4 93.8003 CS2
1 6.1997 STYREHE
100
-------
IDS 01:5297/95/29
6.249
6.308
CHRQI1ATOGRAI1 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 6
REPORT NO' 56
LflSCQ TUBES
FILE
METHOD
0
8992
TIME
TOTAL
AREA
3G1359
COHC
NAME
1
c!
3
4
5
6
•1.
.-,
•-' •
4.
6.
6.
9.
533,-,
Q27
623
249
908
642
348
3242
£11545
1263
333
84579
4
3
4
i
71.
8.
28.
\J
1
5
4
c
c
c
•J
0
c
J
9
1
1
CS£
MM A
STY
100
-------
c. >;> • c. i ? /•
3.028
6.253
c. r
L H S L- U I LI E L i
4.825
CHROMftK
1ft \ ^ fj *
V • 1 £ 0
3GRAH 1
r v
MEMORIZED
CR581 CHROI1ATOPAC
CHANNEL
HO 1
SAMPLE HO e
FILE Ei
METHOD 0002
REPORT HO 54
PKNO
1
£
0
4
5
6
TIME
3.928
4.025
6.253
9.392
9.646
10.128
AREA MK IDHO COMC NAME
1891
£15493 4 £7.6S£3 CS2
1343
w1 v1 0
561788 1 72.1665 STYREHE
1177 £ . 0.1512 CUMEME
TOTAL
782038
1BQ
M
M
U
6
6
10
-------
4 • H H : j y y / /
3.831
— ——
6.256
Ci 'T1 0 0
16.13 "
CHROttftTOGRfttt 1
CR501 CHROllftTQPflC
CHAHHEL HO i
SAMPLE HO Q
REPORT HO 55
:'KHO TIME
1 • 3.831
£ 4.0E8
o b . c jo
4 9.332
5 9.648
6 19.13
J D / c ?
4.923
flEMORIZED
RREh UK
1837
£11219
1£64
378
538755
927
LHSUU 1UELS
FILE 8
METHOD 009S
IDHO COHC MAHE
4 £3.1287 CS2
i 71.7478 STYREHE
2 G.I £35 CUMEHE
TOTAL
75437E'
100
-------
CHROI1ATOGRAM 181 MEMORIZED
43$ 14:66:11
2."SIT
LASCO BAG SAMPLES
£.51?
CR581 CHROI1ATOPAC
CHftMliEL HO 2
SAMPLE NO 9
REPORT NO 53
PKNO
TII1E
TOTAL
AREA MK IDM0
FILE. 9
METHOD Q(
CONC
16506
NAME
2.517
£.608
2.813
14820
1215
471
V
V
1
•-•
L.
32.4217
'7.5783
100
-------
;HROHATQGRAH 101
•"7/65/29 14:01:58
;R5B1 CHROHfiTOPAC
LftSCO BAG SAMPLES
/0-/2-3 -,
£.517
M
M
U
6
8
u
CHANNEL HO 2
SAMPLE NO 8
REPORT NO 5
PKI10
TIME
1 £.517
£ £.667
•o • •:• o 1 ?
,.; L. . y 1».
TOTAL
RREA !1K
15369
1£64 V
510 V
17143
1DNO
FILE
METHOD
COtIC
9
9802
NAME
92.481 METHANE
7.59? ETHANE
100
e
b
-------
DC': Uby
LASCO TUBES
J-II-Z.
4,83
6.25
CHROMflTOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO 8
REPORT NO 48
PKHO
TIME
TOTAI
AREA UK I UNO
FILE
METHOD
CONC
8
8862
NAME
1
c
3
4
5
6
?
1.
1.
£.
3.
-i
O •
4.
b.
533
S98
155
054
462
03
£5
3192
964
949
618
395
210059
1371
\!
217548
1SB
108
CSS
-------
12:31:2697/05/29
4.827
6. £55
CHROHfiTOGRAH 1 lOQRIZEB
LASCO TUBES
Is)
ro
CO
6
6
NJ
CR5Q1 CHROHATOPAC
CHftHMEL MO 1
SAMPLE HO Q
REPORT HO 47
FILE
METHOD
0
9092
PKNO
TINE
AREA MK I UNO
CONC
HA HE
1
£
b1
4
5
6
7
: .1 . 59
1.896
£.154
3.052
3.46
4.027
fa. 255
3231
975
954
G££
405
£11020
1376
TOTAL
£13534
100
100
CSS
-------
!if:iu:3,79?/85/£9
LASCO TUBES
3.825
' .", .*
b.
-------
u
Nl
6
Is)
3.825
6.253
6.923
4.02?
10.1
C.J
CHROHATOGRAH 1 MEHORIZED
CR5G1 CHROHATOPAC
CHANNEL HO 1
SAMPLE NO 0
REPORT HO 45
?KHO TIME AREA UK IDHO
1 3.025 1264
£ 4.62? 208615 4
3 6.253 1963
4 6.9£3 448 3
5 9.647 336572 i
6 ' U0.125 •--,. 813 I
FILE
METHOD
COHC
O
6002
NAME
.38.1766 C;£
9.8819 MMA
61.5927 STYRENE
8.1488 CUMEHE
TOTAL
548??6
-------
11:38:5297/65/29
LASCO TUBES
•~* it-*!
Oi 00
4.Q27
6.256
6.917
18:If?
CHROHATOGRAH 1 I1EI10RIZEB
CR581 CHROMftTOPAC
CHANNEL NO 1
SAHPLE NO 0
REPORT NO 44
FILE
flETHOD
9
8882
PIC HO
1
c
3
4
5
6
7
T
3.
dt
6."
§.
9.
10.
10.
IME
83
027
£56
917
652
137
619
AREA UK
1650
£16909
1331
348
530495
1038 V
442
IDNQ
4
**
1
2
COHC
c'7.
8.
7£.
8.
1547
8435
6718
13
NAME
CS£ ••
MHft
STYRENE
CUHEME
TOTAL
8Q2212
100
K)
NJ
LJ
-------
CHROMAT
1 1 : 11 : 1 c y f ••
3J336
=—
6.25
6.928
OGRAM 1
CR531 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT HO 43
PKNO TIME
1 •'"' 3.036
£ 4.032
3 6.25
4 6.928
5 9.652
6 9.791
7
10.125
TOTAL
4.032
L.
MEMORIZED
AREA h!C
45.83 .,,
£11457
1271
322
557483
4352 V
1483 V
777956
LHblU lUELb , /V»
'
FILE 0
METHOD 9002
IDNQ. CONC NAME
,-' ;"
4 £7.4353 CS£
3 9.0417 MM A
1 72.3299 STYRENE
£ 0.1931 CUHEME
1GO ...
e
IP
t
-------
3.031
6. £55
4.G26
CHROHflTOGRftH 1 MEMORIZED
CR501 CHROHflTOPflC
CHAHHEL HO 1
SAMPLE NO 8
REPORT NO 45
FILE
METHOD
Q
0062
FKHO
TIME
3.031
6.255
9.651
TOTAL
AREA !1I< IDHO
1340
08796 4
1256
34420 1
COHC
NAME
245812
O c; o d p
'.' J • V *T 0
180
STYRE HE
KJ
OJ
6
M
O
u
VI
6
N)
si r
-------
3.831
4,828
6.255
10
10
CJ
6
8
u
•>J
6
NJ
CHROHATQGRAI1 1 . MEHORIZED
CR501
CHANNEL
SAMPLE
REPORT
FKNO
1
£
3,
4
CHROMATQPAC
HO 1
HO 0
HO 37
TIME
3. '031
4.020
6. £55
9.649.
TOTAL
AREA MK
1333
£13£63
1276
35176
£51098
FILE
METHOD
I DUO COHC
4 85.
1 14.
100
0
000£
NAME
S411 CS£
1589 STYRE
e
-------
[39:24:3497/85/29
4.02;
6.242
6.92
i T» ••
i 18-.S33
CHROMATOGRAM 1 I1EMORIZEB
CR5G1 CHRQMATOPAC
CHAHHEL HO 1
SAMPLE HO 8
REPORT NO 36
?KNQ
4
5
6
TIME
3.028
4.023
6.242
6.92
9.64?
10.297
10.553
TOTAL
1247
212730
1262
252
115758
9996
16313
357562
LASCO TUBES
IDHCi
FILE
METHOD
COHC
HA HE
64.7108-CS2
0.8766 11 MA
35.2126 STYRENE
108
-------
39:84:0897/
3.031
-»^—
6.252
6.921
95/29
• 4.026
10'.TfeV
LASCO TUBES
CHROMATOGRAH 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO O
REPORT NO 35
KJ
CJ
6
u
N4
6
PKMO
TIME
TOTAL
fiREA MK- I UNO
FILE
METHOD
CONC
Q002
324086
NAME
i
.-,
c
•-J
4
5
6
.-,
0 •
4.
6.
6.
9.
10.
031
026
252
921
644
126
1269
213531
1261
£60
186764
1001
4
,-,
•-'
1
/•.
c
6 6 .
8.
33.
0.
4054.
flSDS
2G23
3114
r- r- *~i
L- 0 c
!1M A
STVREHE
C LIME HE
190
-------
1.587
3.832
6.242
9.644
4.026
CHROHATOGRAN 1 MEMORIZED
CR5G1 CHROMA TOPAC
Ch'AHHEL NO I
SAMPLE HO 9
REPORT HO 34
TIME
MK IDNO
1.5S7
3.032
4.026
6.242
9.644
1521
457
24S995
1553
1399
FILE
METHOD
CONC
0
0002
NAME
TOTAL £45925
4 99.4227 CS2
1 8.5773 STYRENE
100
-------
o
CJ
VI
6
IS)
)8:£3:3497/05/£9
1.587
3.0£6
4.618
6.£44
10.507
CHROHATOGRAH 1
CR501. CHROHATQPAC
CHANNEL NO 1
REPORT NO 33
MEHQRIZED
PKNO
TIME
AREA MK IDHO
LASCO TUBES
TILE
flETHOD
CONC
O
999£
NAME
e
1
£
3
4
5
6
1.
3.
4.
6.
9.
18.
587
826
01S
£44
637
507
£1
1
1327
397
5147
1283
1031
047£
4
1
99'.
8.
5
4
:• o o
C.-JL.
768
TOTAL
££9658
IBB
-------
26:3497/95/28
3.83
5. £54
6.£33
4.Q£3
CHROttATOGRAtt
CR5B1 CHRORATOPAC
CHANNEL MO 1
SAMPLE NO 8
REPORT NO £33
MEMORIZED
LASCO TUBES
PKHO
TIME
AREA HK IDHO
1
£
3
4
3.83
4.023'
5. £54
6. £33
553
245829
.4322
380
FILE
METHOD
COHC
100
0
000£
NAME
CS2
TOTAL
J51075
190
-------
2.493
CR5B1 CHROHATOPAC
CHANNEL HO £
SAMPLE HO 8
REPORT NO £82
PKNO
TIME
£.493
£.584
£.737
AREA !1K IDHO
17726 1
935 V £
442 V
FILE
HETHOD
COHC
9
eeee
NAME
©
b
94.9386 'METHANE
5.0114 ETHANE
TOTAL
191Q3
100
-------
3.026
5. £49
6. £39
4.015
CHRQI1ATQGRAI1 1 HEHORIZED
CR5B1 CHROHftTOPAC
CHflMMEL MO 1
SflHPLE HO 8
REPORT HO £81.
PKMO
TIME
3.926
4.015
5.249
6.239
TOTAL
AREA MK I BUG
437
£99441 4
3272
£76
£13426
FILE
METHOD
CONC
10B
9
sees
NAME
CS2
190
to
to
u
-------
97/65/2:
El
19:56:16
LASCO BAG SAMPLES
Q\\J
2.492
CR561 CHROHATOPAC
CHANNEL HO £
SAMPLE HO 8
REPORT NO £88
PKNO
1
2
3
TIME
2.492
£.584
£.736
AREA tIK IDNO
17595 1
933 V £
439 V
FILE
METHOD
COHC
9
0Q9S
NAME
94.9397 METHANE
5.0603 ETHANE
TOTAL
18877
190
-------
119:44:4997/05/20
3.03
5. £55
6. £44
6.9
LASCO TUBES
HM-1-2
fti f\
CHROliATQGRAM 1 MEMORIZED
CR5G1 CHROHATOPAC
CHANNEL HO 1
SAMPLE '"0 0
REPORT fifl £79
FILE
METHOD
9
808£
NJ
S)
u
6
M
O
U
VI
6
PKHO
TIME
TOTAL
AREA MK IDNO
1
£
3
4
5
6
?
3.63
4.9£
5.255
6.244
6.9
9.5
9.633
366
£44354
3246
365
537
434
2909
V
25££10
COHC NAME
98/6394 CS£
8.2165 MMA
1.1741 STYRENE
100
e
-------
97/85/29
19:35:14
2.78?
LASCO BAG SAMPLES
2.492
CR581 CHROHATQPAC
CHANNEL NO E
SAMPLE NO B
REPORT ND £78
>KHQ
TIME
2.492
2.585
2.737
AREA UK IDHO
76569 1
3129 V 2
FILE
HETHOB
CONC
Q ;
6082
NAI1E
96.6737 METHANE
3.9263 ETHAHE
TOTAL
88431
108
-------
• 9:£3:5l97/85/£8
4.012
5.£46
6.£37
6.905
,". f .-.
•}. t-o
CHROttATOGRAII 1 MEMORIZED
LASCO TUBES
ftiA
to
to
u
6
to
o
W
X
6
to
CR581
CHANNEL
SAMPLE
REPORT
P.KNO
1
c!
r,
'j
4
5
CHROHATOPAC
HO 1
HO 0
HO £77
TIME
4 . 8 1 £
5. £46
6. £37
6. 905
9.63
AREA UK
£09973
£503
£86
405
£278
I DUO
4
3
1
FILE
METHOD
CONC
8
8002
NAME
TOTAL
£15445
93.7383 C3£
8.1985 UNA
1.8712 STYRENE
198
-------
?:«(:; q.sy/'/t
1.986
3.824
.,. ' •
1 5. £46
6. £38
\ ?-4?|
1
CHROHATOGRAH 1
CR501
CHROHATOPAC
D/C.U
4.813
1 « * W *
hEMORIZEB
CHANNEL HO 1
SAHPLE
REPORT
PKNO
1
£
3
4
:;
0
i
o
w
9
HO 6
HO £75
HUE
1.966
'3.624
4.813
5.246
6.238
6.901
9.478
9.81?
10.27
AREA (IK
388
698
2B2796
3719
264
782596
18876
9696 V
1E326 V
LHbUU lUtitb
FILE 6
METHOD 0802
I DUO COHC NAME
4 ' • 23.53QE CS£
3 79.4198 ntlfl
TOTAL
198335!
166
-------
LfiSCO TUBES.
CHROMATOGRAH 1 MEMORIZED
WARNING HO PEAK
8t41:3897/65/28
LASCO TUBES
1,983
3.8£3
=
5.251
6. £43
4.Q15
9.638
CHRONATQGRAH 1 MEMORIZED
CR5B1 CHROHATOPAC
CHAMHEL MO 1
SAMPLE HO 0
REPORT HO £73
?KMO
1
TIME
1.983
AREA IIK IDNO
331
FILE
METHOD
COHC
NAME
z
3
4
5
6
/
3.023
4.815
5. £51
6.243
6.58?
9.638
749
2Q9356
3962
279
832159
1D55
TOTftL
1847932
£0.0888 CSS
79.818 HHft
8.1012 STYRENE
108
-------
81. 92: 4497/65/29
1.962
3. 822
5. £45
6. £36
4.814
9,633
CHROHATQGRAH 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO £7£
LftSCO TUBES
FILE
HETHOB
9
9992
M/M
to
>o
6
8
6
S3
?KHO
1
c
•J
4
5
6
7
8
TIHE
C. 1.902
.'" 3.922
4.014
5.245
6.236
6.899
9.44£
9.633
AREA tIK I DUO
1192 ;,. '
863
2T3684 4
4708
£35
•286492 3
996
444 V 1
C9NC
42.
57.
6.
6915
£197
0888
NAI
CS£
MH A
STY
TOTAL
508484
100
-------
5. £5
6. £41
o f •:•'
7 • & J »
CHROMATOGRAN 1 MEMORIZED
CR501 CHROI1ATOPAC
CHANNEL HO 1
SAI1PLE HO 8
REPORT HO
PKNO
1
3
4
5
1
TIME
•?82
8£4
088
4
5
6.241
5.25
RREft MK IDHO
£99433
4531
£36
FILE
METHOD
COMC
B
8002
MAHE
43.4£46 CSS
b 6.983
7 9.633
272527
33£
56.5066 UNA
8.8688 STYREHE
TOTAL
489120
109
-------
17:£l:i697/85/£8
4.908
'-' » i -.' >.'
CHROHATOGRAII 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT HO £78
LASCO TUBES
LO&
FILE
METHOD
0
8B8S
W
W
6
o
u
•si
6
10
?KNO
TIME
AREA tIK IDNO
COHC
HfttlE
1.894
784
c
3
4
5
6
7
8
o . U 14
4*8 OS'';*.
5. £44 "
6.234
6.899
9.628
18.188
/OJ
£86567
48£1
£38
£38843
341646
439299
4 jX ', .
i*
^.*
i
i
c
16.855
19.4S33
•"' 7 <*' "^ i! >j
C / . 0 (' 07
35.8449
tlMft
e
1
TOTAL
1£31295
iee
-------
y:4ti:c.jy,'-/t
1.949
J . U 0 0
— — —
• 5.323
6.321
3.033
b/Ub
4.09
C' • J O A
.• * { L.
UKROMATOGRAtl 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
?KHO
1
U
0
4
5
6
7
r
8
9
10
11
12
CHROMATOPAC
HO 1
HO 0
NO 18
TIME
1.949
3.083
4.09
5.3£3
6.321
6.981
3.033
9.72 1
10.211 1
10.527
10.633
10.939
AREA MK
1876
994
192483
5315
307
696263
365
474506
375390 V
1840 V
328 V
231
LHSCO TUBES ^
.
1 U i C i i
FILE B
METHOD G002
I UNO COMC NAME
3 19.6343 UNA
1 41.5S04 STYREHE
2 33.7853 CUMEME
M
M
O
CJ
TOTfiL
3749896
100
-------
9:20:4997/66/66
LASCO TUBES
1.949
3.895
==—
5.325
6.323
4.092
3.0£5
' 11:11!
CHROHftTOGRfttl 1 tOORIZEB
CR581 CHROHATOPAC
CHANNEL NO 1
SAHPLE HO 6
REPORT HO 17
PKNQ
TIME
AREA m IDNO
FILE
METHOD
CONC
8
8002
NAME
1
2
3
4
5
6
7
8
9
18
11
12
1.949
3.895
4.892
5.325
6.323
6.983
8.0£5
9.722
18.213
18.529
18.633
18.941
1937
991
199490
5228
295
675646
349
1419567
1322336 V
1649 V
263 V
195
19.7667
41.5309 STYRENE
38.7924 CUHEHE
'OTAL
J619488
100
-------
/:91:1197/06/86
1.628
3.B83
==—— 4.69
5.333
6.324
6.989
—9.7S4
CHROHATQGRAI1 1 MEMORIZED
CR581 CHROHATOPAC
CHANNEL NO 1
SAI1PLE HO 0
REPORT HO 16
LASCO TUBES
WDA-/3-)
PKHO
TIME
ftREA MK IDNO
FILE
METHOD
COHC
B .
9092
NAME
1
£
•3
O
4
5
6
7
1.688
3.883
4. 09
5.333
6.3S4
6.989
9.724
2993
1506
137917
571
1264
1656
2344£
IO
ro
OJ
6
to
o
CJ
V(
6
M
TOTAL
£19£6G
6.5996 tin A
93.4Q04 STYREHE
10fl
-------
|18: 4153197/96/06
1.63
3.996
LASCO TUBES
4.894
5.33?
6.327
6.983
-?.726
CHROHATOGRAtl 1 MEMORIZED
CR501 CHROtlATOPAC
CHANNEL NO 1
SftflPLE NO' 6
REPORT HO 15
PKHO
TIflE
AREA
IDMO
TILE
HETHOH
COHC
NAME
1
2
•^
>j
4
5
6
7
1.63
3.896
4.894
c; <-,<;->
•J . O O (
6.32?
6.983
9.726
3001
1579
192312
578
1324
1730
24368
TOTAL
224893
6.6295 UNA
93.3705 STYRENE
188
-------
8:21:4597/06/06 LASCO TUBES
1.627
3.1
===a»—
5.325
6.325
— 9.726
CHROMATOGRAM 1
CR501 CHROMATOPAC
CHANNEL NO 1
SArtPLE NO 9
REPORT NO 14
PKNO TIME
1 1.627
£ 3.1
3 4.09 .
4 5.325
5 6.325
6 9.726
4.69
MEMORIZED
FILE G
METHOD 0002
AREA !1!< I UNO CONC NAME
370
343
132701
494
1206
18785 ! 100 STYRE
o
r,
i
KJ
ro
u
u
VI
6
TOT.AL
£04399
100
-------
18s81:5797/96/86
1.6£6
4.091
LASCO TUBES
5.325
6.324
•9.724
CHROHATQGRAH 1 MEMORIZED
CR581 CHROHATOPAC
CHANNEL NO 1
SAMPLE HO 9
FILE
METHOD
0
0002
REPORT
PKMO
1
2
3
4
5
6
NO 13
•'•••TINE
1.626
3.898
4.091
• '5.325
6.324
9.724
TOTAL
AREA IIK I.DNO
954
376
193962
542
1345
21106 1
218284
CQNC
tlntlE
100
100
STYRE HE
-------
17:42:0497/06/96
5.329
6.319
4.Q87
CHROMATOGRftH 1 MEHORIZED
LftSCO TUBES
A/D/W2-'
10
K)
U
6
K)
o
CR5B1 CHROI1ATOPAC
CHAHHEL HO 1
SAMPLE HO EI
REPORT NO 12
FILE
HETHOD
Q
0002
TIME
AREA MK ID NO
COHC
HAHE
4.037
5.329
6.319
133216
476
1132
TOTAL
134825
-------
117:22: 1797/96/86
4. 087
5. 328
6.308
CHROMATOGRAI1 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT NO 11
LASCO TUBES
FILE
METHOD
8
0082
:'KHO
1
u
O
•j
4
C
6
TIME
.087
.328
.388
AREA
185153
465
1129
TOTAL
IDNO
COHC
NAHE
186747
-------
:: 0097/06/06
LASCO TUBES
1' *i?3
c • j c \j
- -
-------
6:41:5297/86
3.
5.324
6.314
6.967
8.823
CHROMATOGRAM
LASCO TUBES
9-13-2.
4.883
1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
FILE
SAMPLE HO 8
REPORT HO 9
flETHOD
9002
F'KHO
TIME
TOTAL
AREA
1
2
3
4
5
6
7
8
9
10
11
12
13
»
1.419
1.624
1.936
2.199
3.092
3.515
4.083
5.324
6.314
6.967
3.028
9.713
10.192
687
6866
1974
2800
1462
830
138673
1378
1556
393
360
22684
783
229645
IDHO
CCNC
HA ME
1.6479 MMA
95.0783
3.2318
STYREHE
CUHEME
100
-------
b « cic» 1 o 9 /
3.097
'".• 0 O C'
5.328
6.322
- 8.629
t
CHROHflTDGRAH 1
CR581
CHANNEL
SftHPLE
REPORT
PKNO
1
£
••'
• 4
5'
6
7
8
9
10
11
12
'66/06
4.093
o • I1 1
MEMORIZED
LftSCO TUBES
i U . C 0 >J
:HROHATQPftC
NO 1
HO 8
NO 8
TIHE
. 3.097
3.S88
4.993
5.328
6.322
6.98
8.929
9.714
10.203
10.525
10.625
10.928
THTAL
AREA UK
773
527
£02811
4389
1515
669425
8437
1778858
1662389 V
995 V
318 V
696
4331134
FILE 8
METHOD 0002
IDNO CONC NAME
3 16.2851 MM ft
1 43.2741 S7YRENE
2 40.4403 CUMEI1E
180
\l
M
M
U
6
M
o
-------
CHROHAT
CR561
t-:0£:£797.
3.697
"' ' *
-------
5:48:9597/96/86
LASCO TUBES
1.948
3.891
e ^5
•J . 0 C
6.388
i!
4.888
;HRGMftTOGRfil1 1 MEMORIZED
CR5B1 CHROMftTOPftC
CHANNEL NO 1
SAMPLE MO 9
REPORT ..HO 6
FILE
METHOD
8
0002
PKHO
TIME
AREA UK IDNO
CONC
NAME
4
5
6
7
8
9
IB
11
1.948
3.B91
4.888
5.38
6.
6.
9,
10.
10,
10,
388
97?
715
£66
52
6£5
19.925
TOTAL
£718
1£54
£18317
6454
372
858883
1797147
1674652
3502
398
864
4563692
19.8166 MMft
41.5063 STYRENE
38.6772 CUHEME
SJ
N>
U
6
NJ
O
u
188
-------
.5:61:4797/06/66 .
1,939
3.68£
• 4.Q78
5.312
6.388
9.783
CHROIIATOGRAfl 1 lOORIZEB
CR5G1 :- CHROJ1ATOFAC
CHANNEL HO "l
SAMPLE HO 9
REPORT NO 4
LASCQ TUBES
?KI10
HUE
1.939
3.082
4.673
5.312
6.388
9.703
TOTAL
AREA !1K I UNO
713
485
£17828 4
2277
967
1338 1
FILE
METHOD
COHC
U
8082
HA HE
223599
99.3932 CS2
8.6868 STYREME
100
KJ
KJ
CJ
-------
il!3c.:4iy//f
1.892
3.816
• 5.241
6.225
7.66
'• lift?
CHROIIATOGRAfl 1
CR5G1 CHRQNATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT NO £89
PKI10 TIME
1 1.892
2 3.816
3 4.887
4 5.241
5 6.225
6 6.S98 1
7 7.66
8 9.63
9 9.S
18 18.87
TOTAL 1
JVdti
4n TI •*
. . 8 0 (
I1EI10RIZED
AREA MK
395
776
£11675
4171
289
682076
411
2668
1293 V
1387
985845
LASCO TUBES
FILE Q
METHOD 8882
I UNO COHC NAME
4 il. 1542 CS2
0 «"' C' C *"' C ~* M M rt
0 O 0 • b C- b f' ll Pi H
1 8.1482 STYRENE
2 8.8689 CUHEHE
198
ma
U
6
SJ
O
U
VI
6
All
-------
KJ
: a : s t
I.
-
• J •
'
1 5.
6.
;' t
:34y//ai/t:u Lttbco TUBES ;
904
008
• 4.008
241
233
662
rN/
10
6
u
SJ
6
IO
CHROHATDGRAI1
CR581 CHRQHATOPAC
CHftHMEL HO 1
SAttPLE HO 9
REPORT- HO 284
HEI10RI2EL
PKHO
T.IHE
AREA UK I UNO
FILE
METHOD
CONC
0
8092
NAHE
1
•'t
3
4
5
6
T
{
5
1 . 904
3.0D8
4.008
5.241
£ •:• o o
OIL. -.' w»
6.898
7.662
9.6S9
TOTAL
391
742
207276
3965
281
1669638
317
£278
1824907
ii.:i 1:1197/85/28
CHROHATOGRAH 1
UARNII1G
,"• (I n ft U A T 1
HO PEAK
MEMORIZED
4 11.3933
3 88.4809
i e.isse
100
LASCO TUBES
C32
MMA
STYREHE
e
-------
CHROMATOGRAN 1 MEMORIZED
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
'I?
c
.-^
0
4
e
•J
6
7
3
CHROMATOPAC
NO i
NO 9
NO ' £98
TIME
3.883
4.8Q6
5. 238
6.225
6.894
9. 624
18.108
10.588
AREA MIC
18838
207994
3364
278
51373
4£55SE
773
435
I UNO
4
A
1
2
FILE
METHOD
CONC
0
Q002
NAME
TfUftl
708628
7.4918 MMA
62.S634 STYREHE
0.1127 CUHEME
100
-------
:c. 14! 9997 A
- 3.QQ2
• 5. £4
6. £31
[ 18,1"^''
CHROHATOGRfttl 1
CR5B1 CHROHATOPftC
CHANNEL NO 1
SAMPLE HO 6
REPORT HO £91
?KHO TIME
1 3.882
2 4.Q87
3 5.24
4 ' fa. £31.
5 6,896
6 9.36?
7 9.627
8 10. i
15/28 LftSCO TUBES /"
4.8137
MEMORIZED
FILE Q
RETROD 9888
AREA !1K 1DNO COHC NAME
11157 :
£13098 4 ..-. £9.4681 CS£
3499 ':/
£93 ' . ^'
54176 3 7.4686 RHA
£48
456713 1 63.8185 STYREME
933 £ S.I £88 CUI1E11E
fttA
M
NJ
u
N
6
TOTAL
748611
106
-------
:4897/85/26
LASCO TUBES
1.397
3.883
fit
4.G87
. c
J .
6.
£38
£3
CHRONATQGRAM 1 MEMORIZED
CR501 CHROHftTOPftC
CHANNEL HO 1
SAMPLE NO 8
REPORT HO 292
PKHO
TIME
AREA MK IDNO
1
f,
C
A
•J
4
C
•J
6
7
8
9
10
1.897
3.003
4^887
5. £38
6.23
6.893
9.367
9.622
18.165
10.582
665
8666
238565
5725
332
48487
4£3
778643
1042
351
V
V
FILE
METHOD
COHC
•? o
c c.
8
eeee
HA ME
4.5479 MMA
72.9778 STYRENE
6.8978 CUHEME
TOTAL
1082308
180
-------
CHROHAT
1.898
• 3.887
-
• 5. £44
6.235
. » . , .> i V i»
l u . i y 6
OGRAM 1
CR5D1 CHROdATOPAC
CHANNEL NO 1
SAtlPLE NO 8
REPORT NO £93
?KMO TIME
1 1.898
E 3.007
£ 4.Q11
4'. 5. £44
5 6. £35
6 b . 9
? 9. 626
8 10.186
4.811
*•»
MEMORIZED
AREA HK
542
7 3 £ 1
210185
-v 48££
£81
40705
651103
888
FILE 6
METHOD 8682
I DM0 CONC NAME
4 £3. £794 CSS
3 4.5884 I1t1A
1 72.1139 STYRENE
£ 8.8983 CUMEHE
ft
w
6
N)
Q
u
e
TOTAL
9158.48
190
-------
i L> u t a
fH
4.684
C >"| *% "1
J . £ 6 i
6.226
-6.89
CHROHATOGRAJ1 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT HO 294
PKHO
TI11E
AREA flK IDHO
FILE
nETHOB
COHC
QB82
MAhE
i
2
3
4
c
•J
6
•?
/
8
3
. 4.Q04
'»'." 5.237
6.226
6.89
9.618' '
9.758
19.892
1565
2-35925
3526
341
26924
241938
1198
552
TOTAL
511961
46.6865 CS2
5.3279 Ht1A
47.8764 STYRENE
0.1092 CUMEHE
198
-------
£3:36:9697/05/29
LftSCO TUBES
3.013
=====
5.24
6.££9
4.808
CHROMATOGRAM 1 MEMORIZED
CR5Q1
CHANNEL
SAMPLE
REPORT
PKNO
1
^
L.
3
4
CHRQMATQPftC
NO 1
MO 0
HO £95
TIME
3.618
4.008
5. £4
6. ££9
FILE
METHOD
AREA ilK IDNO CONC
481
£11315 4 199
3214
£81
9
0002
NAME
CS2
(O
N)
O
w
vj
6
KJ
TOTftL
100
-------
4.064
C •"• ^i £
J t 10 fa
CHROHATOGRftH 1 I1EHORIZEB
;R5G1 CHROIIflTOPftC
;HftHHEL -HO 1
5AHPLE HO 0
::=ORT HO £96
FILE
METHOD
r'KHO
TIME
AREA MK IDHO
"COHC
NAME
3.015
4.084
5. £36
6. £27
476
£11406
3185
£79
TOTfiL
£15347
1D9
100
r c- o
'-• Ou
-------
90s 16:5497/05/21
3.G15
5. £39
6. £3
. 9.624
4.GG6
CHROflATOGRAM 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE NO 8
REPORT HO £97
LftSCO TUBES
A/M-5-/
FILE
METHOD
6002
.73
PKNO
TIME
AREA MK ID HO
219693
CQNC
HA (IE
1
£
3
4
5
3.015
4.006
5.239
6. £3
9.624
T rt T A I
575
£14993
3142
£91
697
4 99.6769
1 0.3E31
180
N)
N)
Cj
6
8
6
N)
-------
3.814
i '
•-' i C k> ••
6. ££6
9.619
.CHROI1HTOGRAI1
CR5B1 CHROtlATOPAC
CHANNEL HO 1
SftHPLE HO 9
REPORT HO £98
4.665
e
HEHORIZED
PKNO
TIME
TOTAL
FILE
METHOD
0
9G62
AREA UK IDMO
1
u
•-.
4
5
3.014
4.005
5. £37
b.££6
9.619
559
£11956
307£
£8G
65£
216519
CONC HAKE
99.6934 CSS
6.3066 STYRENE
180
-------
LftSCO TUBES
4.908
5. £33
6. ££9
6.896
CHROMATOGRAM 1 MEMORIZED
CR591 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO
£99
FILE
METHOD
8
B80£
PKNO TI"E AREA MK IDNO
1 1.378 ?;??
£ 1-577 6875
3 1.38 £407
COHC
NAME
4
5
6
7
8
Q
10
11
£.135
3.019
3.439
4.008
5. £33
6. ££9
6.896
9.617
£479
£664
10£4
£155£S
40£0
610
1860
£5154
TOTAL
263438
88.8622 CSS
8
§
u
SI
6
I1I1A
10.3709 STYREHE
108
-------
6.896
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 300
PKNQ
1
£.
•*!
4
5
6
7
8
9
10
11
TH1E
TOTAL
AREA UK IHHO
1.373
1.577
1.881
£.137
3.008
3.437
4.605
5. £39
6. £17
6.896
9.6£
865
6771
£365
•24 £4
£614
990
£1£915
3901
682
1798
£4£21
FILE
METHOD
COHC
0
000£
HA HE
i'59465
39.1184 CS2
0.7524 MflA
10.1372 STYREHE
100
-------
3.945
6.279
6.945
4.Q46
CHROMATOGRfiM 1 MEMORIZED
CR5D1 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 9
REPORT HO 109
PKHO
1
n
2
3
4
j
TIME
3.945
4.046
6.279
6.945
9.671
AREA
3128
193984
1148
426
77397
FILE
METHOD
COHC
NAME
'7 1.3697 CS2
0.1547 MM A
£3.4757 STYREHE
276078
106
-------
3.845
6. £67
4.845
Q.6CO
CHROHATOGRAH 1 I1EMORIZED
CR5B1 CHROHATOPAC
CHANNEL HO 1
'ILE
SAMPLE NO
REPORT HO
FKNO
0
99
TINE
AREA UK IDHO
1
£
3
4
5
3.045
4.045
6.267g;,
6.942
9.669
TOTAL
3818
£18948
1428
514
96572
321280
METHOD
CONC
Q002
NAME
69.£798 C3£
0.1627 11HA
38.5575 STYRENE
100
KJ
KJ
U
6
N)
o
U
vj
6
SJ
-------
6.273
I
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL.NO 1
SAMPLE HO 0
DEPORT HO 98
PKNO TIHE
1 .
1 1.917
4.G46
3 5.287
4.
fa.. 278
fi D r f- IA
H K L H f 1
247
223085
1985
1459
FILE
METHOD
K IDNO CONC
4 1Q0
0
0002
NAME
CS2
TOTfiL
•iee
-------
Z ••£.'! 97/05/23
1.917
5.288
6.278
4.848
i
:HROMATQGRAN i MEMORIZED
CR501 CHROMflTOPflC
CHANNEL HO 1
256266
LASCO TUBES
SAMPLE
REPORT
PKNQ
1
C
3
4 •••.'
NO 0
NO 97
TIME
1.917
4.848
5.238
6.278
AREA
£43
£22613
1962
1442
FILE
METHOD
MK I DUO CONC
4 199
N)
10
LO
6
M
O
NAME
CS2
IflFi
e
-------
[15: £3: 3397/95/23
3.847
6.266
4.037
C.HROMATOGRAM 1 MEMORIZED
CR5G1 CHROMATOPAC
CHANNEL HO 1
SAMPLE NO 8
REPORT HO 96
PKNO TIME
1 1.395
£ 1.597
3 1.905
4 £.164
5 3.047
t. 4.G37 1
AREA
464
££33
668
679
1531
91395
LflSCO TUBES
IBNO
FILE
METHOD
CQNC
0
OQ92
NflME
94.4804 CSS
-------
9.664
CHROI1ATOGRAH
tOORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKHO
1
2
•^
•j
4
5
6
7
1
8
CHROI1ATOPHC
MO 1
HO 8
HO 95
TltlE
.1.397
1.6
1.908
2.158
3.942
.4.845
6.274
9.664
AREA UK
571
2773
831
852
1918
220397
1525
14432
IDNO
4
1
i
TOTAL
FILE
tlETHOB
COHC
8
0BB2
HAME
70,
544
6.1455 STYREHE
243298
10R
-------
l§:i§3
CHROHftTOGRftM 1
CR5B1 CHROHATQPftC
CHANNEL NO 1
SAMPLE HO 9
REPORT HO 94
MEMORIZED
PKNO
TIME
AREA UK I DUO
FILE
METHOD
COHC
6
0992
NAME
1
2
3
4
5
'k:
?.:
8
9
18
11
12
1.383
1,59?
1.906
2.165
3.056
4.Q4
6.266
9.3
9.4
9.655
18.138
10.455
316
1826
407
328
556
££1848
1564
21?
1316
668639
3476
4E5
V
V
( t
V
1
2
£8.2204 CS2
79.4616 STYREME
B.318 CUMEME
TOTflL
1189111
108
-------
4:01:3697/05/23
LftSCO TUBES
3.845
6. £57
4.831
|T| i...
1§:
CHROI1ATOGRAM
MEMORIZED
CR501 CHR6I1ATOPAC
CHANNEL HO 1
SAMPLE HO 8
REPORT NO
Q2
.• wl
KHO
TIME
1
^1
c
r,
Cl
4
5
6
7
8
9
10
11
1.391
1.593
' 1.892
£.15
3.Q45
4.031
6. £57
9.404
9.651
10.135
19.442
347
2613
451
363
580
£30969
1664
1229
921317
2277
484
TOTAL
1161635
K>
o
AREA HK IDHO
FILE
METHOD
COHC
8
8802
NAME
£0.0007 C32
79.802 STYRENE
B.1973 CUMEME
100
1
„->
-------
3.837
6.245
Q.Slfi'J
4,823
u
6
8
u
NJ
6
NJ
CHROMATOGRAH 1 HEHORIZED
CR5B1 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 6
REPORT HO 88
PKNO
1
2
3
4
5
6
7
8
q
18
11
12
;^ U 0 ft "'
TIME
TOTAL
AREA HK IDHD
FILE
METHOD
CQNC
0
9882
NAME
e
h
1.375
1.588
1.883
2.142
3.037
4.B23
6.245
9.283
9.383
9.638
1.0.122
10.439
3£2
1865
418
340
542
288725
1588
253
1238
885718
2305
421
£9.4813 CSS
79.3122 STYREME
0.2864 CUMEHE
1123735
188
-------
3.032
=^— »
6,241
000 -
1
CHROHATOGRAtl 1
CR5B1
CHAHHEL
SAMPLE
REPORT
FKHQ
1
•-.
•~i
•j
4
5
f,
7
r,
0
9
• 10
11
CHROIIATOPflC
HO 1
HO 0
HO 8?
TIME
1.375
1.586
1.883
£.149
3.832
4.698
6.241
9.39
9.637
10.12
19.425
4.008
MEMORIZED
AREA MK
301
1691
369
301
467
o n =; 7 o =;
u :.< -J t u -J
1328
1284
739473
2211 V
391
FILE 0.
METHOD 0002
IDHO COHC NAME
4 £1.7194 CS£
1 73.0473 STYRENE
£ 0.2333 CUMEME
TOTAL
953599
189
-------
38:52:5497/05/29
3.825
6. £ 4 8
4.G23
LASCO TUBES
CHRQHATOGRAM 1 MEMORIZED
CR581 CHROHATOPAC
CHANNEL NO 1
SAHPLE MO 8
REPORT HO 27
r'KNO
TIME
TOTAL
AREA HK I UNO
FILE
METHOD
COHC
0802
HANE
1
2
.•*
0
4
5
6
3.Q25
4,033
6.243
9.639
1 13. 108
10.594
23.G0
228085
1346
291439
632
2121
4
1
2
42.9631 C32
56.9835 STYREHE
G.I 233 CUHENE
517972
100
to
IS)
CO
-------
3,8£4
6.£46
4,021
CHROttATl
ie.i32u%
JGRAH 1
3 -•'. uuj." " '•
I1EHORI2EB
CR501 CHROttATQPAC
CHANNEL
NO 1
SAItPLE HO 9
FILE 9
METHOD i3oea
REPORT NO 26
PKNQ
i
2
3
4
5
.*
0 ,
TII1E
3.824
4.821
6.246
A A ri n
? • O 0 O
9.639
. 18.122
AREA MK I DM0 COHC HAHE
• 2234
215086 '4 43.7715 CS2
12S8
723
275585 'V 1 ...-. 56.8852 STYRE
784 2 -8. 1433 CUHEP
e
TOTAL
495611
-------
3.022
6.248
6.908
4.022
CHROHflTOGR«n i MEMORIZED
CR501 CHROtlATOPAC
CHANNEL NO
SAMPLE
REPORT
PKNO
1
.^
c
•T
0
4
.
6
NO 0
HO 25
TIHE
•1.589
3.022
4.022
6.243
6.903
9.641
TOT A i
ARErt MK
364
3343
215152
1273
337
33335
FILE o
HETHOD OQGc
*MO CONC M
.4
4 . 71.9755 C32
.».
••' '5. 1295 nnfl
1 '•-(•>--_
1 c'7.yy5 sjy
303910
108
M
U
6
-------
J:OC::L. 13 :».•'.'
1.539
3.823
r •
6.247
6.515
1§M2§U
CHROttATOGRAfl 1
CR581 :HROHATOPAC
CHANNEL NO 1
SAHPLE HO 8
REPORT HO 24
r'KHO TIME
1.. 1.539
2'' 3.023
3 4.022
4 6.24?
5 6.915
6 9.638
7 9.775
3
18.123
TOTfiL
J3/iiB
4.822
MEMORIZED
AREA flK
429
3871
233355
1465
441
98446
2755 V
463
341725
LH5UU iUJfLS
FILE 8
METHOD 8882
IDNQ COHC NAME
4 7G. 1336 CS2
3 G.I 3 25 MM A
1 29.5452 STYRENE
2 8.1388 CUMEME
18Q
e '
b;
ulff
-------
>-3; 32:1397/135/28
LrtSCO TUBES
li!
3.833
4.822
V S.Sil
CHROHATOGRffl?
flEHQRIZEB
CR591 CHROHATOPAC
CHANNEL 110 1
SANPLE
REPORT
,'KNQ
1
2
3
4
5
6
7
3
9
19
11
12
13
14
HO 9
HO 23
TIME
1.375
1.5S7
1.833
2.15
3.833
' 4.Q22
6.24?
9.283
9.333
9.639
19.12
18.439
1Q.694
18.894
AREft UK IBNO
233
2237
585 V
56Q
213467 4
1439
349
1166 V
1281618 1
3473 2
935
6493 V
922 V
FILE
METHOD
COHC
8
Q8Q2
NAME
15.8481 CSS
84.7067 STYRENE
0.2452 CUHEnE
M
SJ
TOTAL
1433965
189
-------
l£i9517/05/23
LflSCO TUBES
-1
{
N>
W
S <
o
OJ
:.Q42
4.826
CHROHATOGRAH
MEMORIZED
CR5Q1
CHAMNEL
SflttPLE
REPORT
PKNQ
i
.«i
C
44=
5
6
7
8
9
18
11 •
12
13
14
CHROHATOPAC
HO 1
HO Q
110 £8
TIRE
1.375
1,539
1.395
£.142
3.042 •
4.026
6.252
9. £'36
9.337
9.644 1
10.133
18.441
10.6Q6
19.83?
AREA
261
2432
542
432
618
227879
1557
243
• 1172
316659
3147
138Q
5545
1927
m IB HO
FILE
METHOD
COHC
8
8062
HAHE
14.6764 CS2
34.7938 STYREME
8.5247 CUHEHE
TOTAL
,567936
10Q
-------
£3:12:
LASCO TUBES
bill
z:!«
3.842
:" " "•
6.252
1-J
KJ
to
a
US
Nl
4.026
CHRQHATOGRAH 1 MEMORIZED
e
CR581.
CHANNEL
SAMPLE
REPORT
PKNO
1
•"li
c
3
4
5
6
*)
3
9
18
11
12
13
14
CHROHATOPAC
MO 1
NO e
MO £2
TIME
1.375
'1.539
1.395
£.142
3.842
4.026
6.252
9.296
9.39?
9.644 1
18.123
18.441
1Q.686
18.39?
AREA
261
£432
542
432
619
£27879
155?
243
1172
316659
3147
1383
5545
182?
UK
v
V
V
V
DNO
FILE
METHOD
COHC
8
13882
NAME
14.6764 CS2
34.7933 ST
9.524?
YRENE
CUHEME
TOTAL
1567936
188
-------
•:•. •:• c.
6.254
4.827
I"!?-'
* 645
18:3??
CHROMATOGRAM 1 MEMORIZED
CR581 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 21
F'KNO TIME AREA UK I UNO
1 3.832 1378
2 4.827 213998 4
3 6.254 .,1258
4, 9.645 23751 i
5 18.337 3686
6 18.873 2296
FILE
METHOD
corn:
0
OQ02
MA ME
88.1556 CS2
11.8444 3TYREHE
TOTAL
251265
108
-------
4.826
— *-. 645
19:218
CHRQHATOGRAM 1
MEMORIZED
CHRONATOPAC
CHAMMEL MO 1
SAMPLE MO
REPORT MO
3
PKMO
TIf1E
MK
1
0
4
5
6
3.031
4.826
6.252
9.645
18.302
10.698
1393
217331
1276
2891Q
3370
3391
•' i v vv I 'J * L 0
RE-to-1 a
FILE
METHOD
CONC
0
0882
NAME
33.2355 CS2
H.7145 STVREME
TOTAL
2567
1GG
-------
11J D c. 0
l.i
1:1
.1 r, f> ^t
t • y 11
6.249
6,968
CHROHATOGRAtt 1 MEMORIZED
CR581 CHRGHATOPAC
CHAMMEL MO 1
3AHPLE MO 0
REPORT HO 19
?KHO
TIHE
[OTAL
AREA MK I DUO
FILE
METHOD
COMC
8
8092
HA HE
1
2
0
4 ',
s £:•;
6 ""''
r'
3
9
10
1.375
1.586
• 1.394
, 2.149
.;•' 4.022
' . 6.249
6.903
9.643
' 9.316
10.226
•i i rt
Of 0
2399
333
267
216961
139S
362
117551
3325
5973
349497
63.6526 C32
8.1062 fI
34.4373 STYRENE
1.7539 CUMEHE
100
1-0
to
OJ
6
-------
i :>
1Q.445
CHROMATOGRAH 1 MEMORIZED
CHROI1ATOPAC
CHANNEL MO 1
SAHPLE HO 13
REPORT HO 18
r'KNO
1
o
-J
4
5
6
7
3
q
TIHE
AREA riK I DUO
1.375
1.537
1.395
2.142
4.019
6.247
6.915
9.639
10.445
366
£312
367
251
209950
1299
339
1127Q7
3063
FILE
ilETHOD
COHC
0
9662
HAHE
TOTAL
330660
65.Q01
0.1043 HHA
34.8942 STYREHE
100
-------
4.02:
5.263
6.249
18.717
CHROMATQGRAM 1
CR581 CHRQMATOPAC
CHAMMEL MO 1
SAMPLE MO 0
REPORT MO 17
MEMORIZED
PKNQ
TIME
1
2
3
4
5
6
. 4
5
6
9
q
10
.023
.263
.249
.635
.949
.717
213119
323
1237
3285
5322
1652
22;493S
FILE
METHOD
9
0802
AREA MK IDHO
com: MANE
93.432 CS2
1.513 5TYREME
100
PO
fO
CJ
6
>O
O
CJ
,,-tlf
-------
5.264
6.248
18:
CHROMATOGRAM
4.025
1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT NO 16
PKNO
TIME
AREA UK I UNO
FILE
METHOD
CONC
0
0002
MAI1E
1
2
3
4
'5
'£
7
3
4.025
5.264
6.248
9. 1
9.48?
9.64
10.501
1Q.87S
23Q150
369
1430
2321
2720
502
2319
£265
TOTAL
S4E878
99.7323 CSS
0.2177 3TYREI1E
100
-------
: U : D U • no? / ••
p===="—
6.248
6.915
[ J'.IBI
1 11:^3
CHRQHATOGRAH 1
CR5Q1 CHRQHATOPAC
CHANNEL HO 1
SAHPLE NO Q
REPORT MO 15
?KHO TIME
1 4.Q24
2 6. £43
3 6 . 3 1 5
4 9.39£
5 '5.64
6 10.008
7 10.357
3 10.723
JD/sa
4.Q24
riEMORIZEI)
AREA MK
£13646
1274
437
£942
7936 V
7222 V
3739
£ 1 08 V
LflbUU lUULS
FILE 3
METHOD . 8632
ILHO. COHC HA
'4 96. 3Q32 CS2
3 9V214-7 MM A
1 3.4322 STY
o
i
TOTAL
£44357
100
-------
it), o U > o u. ; i- -•'
.
6.247
6 .914
1 ill
CHROMATOGRAM 1
CR5Q1
CHANNEL
SAMPLE
REPORT
PKNQ
1
.2
:3
4
5
6
7
3
9
18
11
3HROMATOPAC
MO 1
NO 8
NO 14
TIME
4.022
6.247
6.914-,-
3.426
3.93
9.233
9.639
9.863
19.139
19.531
10.345
TOTAL
4.022
MEMORIZED
AREA MK
211942
1224
.,4:51
3565
4467
50SS V
18241 V
9262 V
5343 V
4356 V
1567 V
253889
LrtoCU TUBES
I
FILE 8
METHOD • 8962
i DUO cone HARE
4 92.7612 C32
3 9. 1972 MMA
1 4.4322 STYRENE
2 2.5594 CUMEHE
108
-------
i U : 1 U : 1997 / 0
F=
6.253
ft <-, r-, ^.
0 • 0 C £
. A ii S '%
! ll\$l$
t?: **5
1 lo.yog
CHROMATOGRAM 1 M
CR581 CHROMATOPAi;
CHANNEL NO . 1
SAMPLE NO 8
REPORT HO' 13
?KRO TIME
1 4.026 2
£ 6.253
3 3.322
4 9.453
5 9.733
6 10.023
7 10.354
3 10.908
5/23
4.026
ET10RIZED
AREA [1K
13314
1245
5332
1925
6136 V
8650 V
3730
1489
LASCO TUBES
FILE 0
METHOD 0002
I UNO CQMC MAHE
4 93.5175 CS2
1 2. 6 'i 81 STYRE
2 3.7923 CUMEM
A//)/)-?-/
o
• »A
o
KJ
KJ
bJ
TOTAL
241872
100
-------
4.0S4
LASCO TUBES
l! !!?
lfl.682
CHROMAT013RAM
1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE MO 0
REPORT HO 12
PKMQ
TIME
TOTAL
AREA MK UNO
1
2
3
4
5
6
(
8
9
10
4.024
6.242
3.632
9.029
9.3
9.533
9.64
9.33
10.11?
10.632
215093
1270
7305
12722
10663
4330
2765
10510
3229
2755
276646
FILE
METHOD
CONG
0
0002
MA ME
93. 1475 CS2
2.0915 STYRENE
1. 1972 STYRENE
3.5637 CUflEIIE
100
-------
3. Q£4
6. £45
4.819
9. 184.,-.^.-,
Hi HI
CHROHATQGRAH 1 flEMORIZEII
CR581 CHRQttATQPAC
CHANNEL MO 1
SAttPLE NO 0
REPORT HO 11
PKMO
TIttE
TOTAL
AREA t1K I DUO
1
2
••}
4
c1
•J
6
7
3
9
1Q
3.Q24
4.019
6.245
9.134
9.433
9.637
9.915
18.175
18.422
10.652
1763
21Q767
1235
1G59
2875
357146
3053
9106
5121
6750
603073
FILE
METHOD
CONC
0
OGG2
o
o
:Q
MAI1E
61.3951 STYREHE
1.57S1 CUflEME
CJ
6
Is)
o
CJ
V4
6
to
180
-------
6.244
4.019
ail.......
iS'Ilf
i '3 . C C' -J
CHROMATOGRAM 1
MEMORIZED
CR581
CHANNEL
SAMPLE
REPORT
PKNQ
1
£
•j
4
5
6
7
3
9
18
11
12
CHROMATOPAC
NO 1
HO 8
HO 18
TIME
3.Q25
4.819
6.244
9.817
9.292
9.392
9.496
9.636
9.983
10.103
18.483
18.665
AREA
£062
£33263
1428
17S8
£986
£823
3969
423253
5685
4727
3353
1341
FILE
METHOD
C-OHC
8
0882
HAI1E
35. £765 CS2
64.0836 STYREME
8.7149 CUHEHE
TOTAL
635388
188
-------
18:49:3397/05/28
3. 829
6.24£
6.917
LflSCQ TUBES
4.62*
CHRQMATOGRAtt
1 MEMORIZED
CR581 CHROMATOPAC
CHAHMEL HO 1
SAMPLE HO 8
REPORT HO 9
r'KMO
TIME
1
il
3
4
5
6
7
3
9
18
11
12
13
14
3.829
4.326
6.242
6.31?
3.799
•3.067
•3.275
9.375
•3.433
•3.64
10.122
19.363
10.5131
10.773
2044
230312
1333
3G2
1095
563
1591
1091
1325
568327
1757
219£
4047
3948
TOTAL
AREA IIK OHO
4
3
1328349
FILE
METHOD
CO HC
0
0002
HA ME
23.7459 CS£
Q.8377 tlttA
78.9971 STYREHE
0.2193 CUflEflE
CJ
6
M
O
CJ
•vj
6
ro
108
-------
18: £-9: 3197/95/23
LASCO TUBES
3.Q28
6.£46
f,. 913
ME -
6
N>
o
GJ
•M
6
K)
4.824
CHROHATOGRAH 1 MEMORIZED
CR5Q1 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO a
REPORT HO 8
FILE
METHOD
9
8QQ2
f'KNO
'If1E
AREA MK IDHO
cone
1.
9 ''•
O
4
5
6
7
3
9
10
3.328
4.824
6.246
6.913
9.033
9.298
9.275
9.39
9.634
18.116
2303
241332
1532
353
499
330
490
1431
644476
1379
!7.£36 CS2
8.8484 MMA
72.5684 STYREHE
Q.I552 CUHEHE
TOTAL
394735
188
-------
a. 021
5 . £65
6.233
6.9
4.019
CHRONATQGRAN 1 MEMORIZED
CR581 CHRONATOPAC
CHANNEL NO 1
SAMPLE NO O
REPORT NO 7
>5KHO
TINE
TOTAL
?3874
•J u. C
JUNO
3.021
4.019
5.265
6.233
6. 9
5.633
10.114
2337
215505
436 ,
1303
? 7 9
189765
444
3
1
2
FILE
METHOD
COMC
0
0302
NANE
6.2453 MNA
31.7377 STYRENE
0.1399 CUMENE
o
10G
.f.
-------
4.815
5. £61
6. £39
CHRQHATQGRAH 1 MEMORIZED
CR591 CHROMATOPAC
CHAHNEL HO 1
SAMPLE HO 0
REPORT HO 6
PKNQ
TIME
AREA MK. I UNO
FILE ,
METHOD
COHC
8
0002
MAHE
1
2
3
4
.5
6
7
i
•1
4
5
6
6
Q
10
.003
.015
.261
.239
.986
.632
. 103
2353
215773
426
1295
972
182895
1302 V *•
4
3
1 .
2
67.
8 .
3 1',.
8.
3993
3836
3,984
4867
CS2
tin A
STYRENE
CUHEME
TOTAL
324716
190
-------
17:29:'G697/C
1.892
7=
=; •:• f. •:•
•J • L. -J L.
i {• -' '' O
C' • L. ij L1
/ . 'd
r
1 fl C' ° 1
CHROnATOGRATf u" 1
CR581 :HROMATOPAC
CHANNEL HO 1
SAMPLE NO 9
REPORT MO 5
:'KMO TIME
1 1.332
£ 4.015
3 5'*2S£
4 6 .'£33
5 6.931
6 7.2
7 9.631 1
3 19.112 1
9 10.831
15/28 LAS CO TUBES
4.015
-•• • '-' J * - ...
i W • A * U
MEMORIZED
:
FILE 0
METHOD Q00£
AREA MK IDHO CONC MftME
243
21SS23 4 4.7/34 C3£
457
1304
919229 3 £0.0 7 £5 Mil ft
1998 V
791912 1 39.129 STYRENE
649534 V 2 36.02 CUMEME
599
ro
TOTAL
4533195
199
-------
£0:34:0997/85/29
1.593
LASCO TUBES
10-11-1
:.039
5. £68
6. £54
6.921
4.0 £-6
p+f
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 85
PKNQ
4
5
6
7
8
9
TIME
1.593
3.039
4.Q26
5. £68
6.254
6.921
9.493
9.647
18.117
AREA !1K IDHO
1 O O O
332
217201
45£
1471
356
£87
326285
560
FILE
METHOD
COHC
0
000S
NAME
39.7511 CSS
Q.0652 MMA
60.9812 STYREHE
0.1925 CUMEME
TOTAL
550281
100
-------
4.028
6.254
CHROMATOGRAM
1 I1ENORIZEB
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE HO Q
REPORT NO 86
PKNO
' TIME
4.QS8
6.254
9.645
TOTAL
AREA MK IDNO
£10741 4
1277
461442 1
FILE
METHOD
COHC
0
0002
NAME
673463
31.3518 CS£
68.648£ STYRENE
100
OJ
6
CJ
VI
6
to
-------
cl: 14:4697/85/29
4.83
6.255
.' % 'J T '_'
CHRQMATQGRAM 1 MEMORIZED
CR5G1 CHROHftTOPAC
CHANNEL HO
SAMPLE HO
REPORT'"MO
?KMO
1
0
37
TIME
LASCO TUBES
AREA ilK IDHO
FILE
METHOD
CONC
T£&&oL
$^
102,
I
D
80Q2
HAME
4.83
6.255
9.646
TOTAL
235576
1543
553321
4
1
796448
O Q O il 1 c* f- C- O
u 3 • »j O I ^' '-f -w1 L.
70.1335 STYREHE
189
-------
4.026
6. £42
CHROMAT
3GRAM 1 MEMORIZED
CR591 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 8
TILE 9
METHOD 0002
REPORT HO 88
PKNO
1
2
TIME
4.026
6.242
9.64
TOTAL
AREA MK IDN9
4
1
750316
211534
1277
537585
CONC NAME
23.2407 C52
71.7592 STYRENE
188
to
to
w
6
to
o
-------
LI :55:0597/05/29
4.QS4
6.249
CHRQHATQGRAH 1 MEMORIZED
LASCO TUBES
mi
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO Q
REPORT HO 89
•KNQ
1
TIME
4.024
6. £49
9.633
TOTAL
FILE
METHOD'
8
Q0Q2
AREA MK IDHO
209882 4
1245
5228G5 1
CONC NAME
2S.5983 CS2
71.4012 STYREHE
166
-------
4.024
£47
CHROHATQGRAH 1 MEMORIZED
CR501 CHROJ1ATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 90
FILE
METHOD
0
QDB2
PKNO
i
c
3 '
TIME
4.Q24
6.£47
9.638
TOTAL
AREA t1K I DUO
4
1
977606
218642
1351
757613
CONC NAME
22.396 CS2
77.684 STYREME
180 '
-------
u H s u U I u b L b
,823
6.24?
CHROHATOGRAH 1 MEMORIZED
CR581 CHROMATOPAC
CHAHMEL NO 1
SAMPLE NO 0
REPORT NO 91
PKHO TIME AREA t1K I UNO
1 4.823 214071 4
£ 6.£47 1317
FILE
METHOD
COHC
250.7
8
Q98S
NAME
•3 O O 1 O 1 r C 9
C C . C 1 O 1 '-• J u
9.639
TOTAL
749641
965829
77.7869 STYREHE
188
-------
- I
1.591
3.019
5.£63
6.243
6.915
O •? 0 O . ...
4.923
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHAHMEL HO 1
SAMPLE HO 0
REPORT HO 92
PKMO
1
£
3
4
b
•7
i''
B
q
19
TIME
1.591
AREA
14££
IDNO
FILE
HETHOD
COHC
0
09Q2
HA HE
3.019
4.023
5. £63
6.248
6.915
9.393
9. &4£
10.117
19.447
8733
£28040
896
1475
702
366
56Q983
2072
337
28.G736 CS£
Q.0B95 MtIA
71.57E6 STYREHE
8.2643 CUMEME
TOTAL
7970E5
198
-------
CHROMAT
CR581
CHANHEL
SAMPLE
REPORT
PKMO
1 •
c. •
3 -;
4
5
6
7
8
9
18
1.589
- 3.019
- • i . f
5.25
6.246
6.91 3
o •:> o o
OGRAH 1
CHROMATOP
HO 1
HO 8
NO 93
TIME
1.589
3.019
4.822
5.25
6.246
6.913
9. 333
9.637
18.108
18.437
— 4.B22
MEMORIZED
AC
AREA MK
1361
8250
218218
836
1373
644
272
516297
984
481
FILE 8
METHOD . 0802
I DM0 COHC NAME
• -. 4 28.3697 CSS
3 8.8885 (IMA
1 78.9867 STYREHE
2 0.1351 CUMEHE
r
TOTAL
749629
188
-------
23:35!£097/@5/£9
• 1.588
- 3.015
• 4.02
5. £61
6. £46
6.913
a o Q d.. , „. ,.
LftSCO TUBES
10.1£3"v"
CHROMATOGRAH 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKMO
1
£
2
4
5
6
7
8
Q
CHROMATOPAC
HO 1
NO 0
HO 94
TIME
1.588
3.015
4,62
5. £61
6. £46
6.913
9.394
9.639
10.123
TOTAL
AREA MK
1502
9280
216749
551
13£4
685
320
461321 V
1750 V
693482
ID HO
4
3
<
•~,
i_
FILE
METHOD
CONC
6
6B8£
NAME
31.S5-12 CS2
8.1007 MMA
67.791 STYRENE
0.2572 CUMEME
o
100
-------
5.
6.
6.
o
i , u c t
£65
249
9Q8
10. 1 £2 " u"Ti
Kl
K>
U
6
XI
6
CHROHATOGRAH 1 MEMORIZED
CR5G1 CHRQMATOPAC
CHAMHEL NO 1
SAMPLE MO 9
REPORT NO 95
PKNO
TIME
AREA IIK I HMO
FILE
METHOD
COHC
0
8082
NAME
1
2
.-4
O1
4
5
6
7
8
9
1.588
3.'017
4.0£4
5. £65
6. £49
6.908
9.397
9.641
10.122
1497
9£9£
217233
55£'
1331
695
£76
461S86
1157
TOTAL
693319
31.9286 CS2
Q.1822 MHA
67.7992 STYRENE
0.17 CUHEME
100
-------
1 1> • i J • O C ? f
1.586
— 3.013
====—
5. £5
6. £47
6.914
Q '.< * '..
f 10.119
CHROMATOGRAM 1
CR5Q1
CHANNEL
SAMPLE
REPORT
PKNO
1
o
3
4
. 5
6
7
8
9
•US/' 0' U
- 4.G22
.• « *-' ^' .•'
MEMORIZED
LHSLU iUBLt> .. -^
/V\K
' VC-,
CHRQMATOPAC
HO 1
MO 0
MO 96
TIME
1.586
3.813
4. 0££
5. £5
6. £47
6.914
9.383
9.639
10. 119
TOTAL
AREfi MK
1123
14EB6
£15456
931
1336
1E67
492
1269876
£365
1507052
FILE 0
METHOD OOS£
I DUO COHC . NAME
4 14.4702 CSS
3 O.OS51 I1MA
1 85. £859 STYREHE
£ 9. 1583 CUMEME
100
to
N>
CJ
-------
10:35:3297/05/39 .
1.589
LASCO TUBES
CJ '
V4
6
N)
r- 3.014
5.25
6.246
6.911
Q 9 •? B
4,023
CHRQMATOGRAM 1 MEMORIZED
CR581 CHRQMATQPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 97
FILE
METHOD
TIME
AREA MK IDHO
CONC-
HA ME
1
£
3
4
5
b
?
8
9
IB
11
1.5S9
3.814
4.G23
5.25
6.246
6.911
9.275
9.389
9.636
1Q.116
10.436
1 •*' c o
i •_' -j •-'
17258
245613
1141
16£6
1549
273
808
1555674
3563
£30
1
£
TOTAL
1329134
13.5968 CS2
Q.G858 MMA
36.1202 STYREHE
0.1972 CUMEME
100
-------
5. £64
6.247
6.914
7.957
4.924
CHROMATOGRAM 1 MEMORIZED
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
••i
L.
3
4
C
6
i"
's
9
18
11
CHRQHATOPAC
HO 1
HO 8
HO 98
TIME
1.539
3.818
.4.624
5.2.64
6.247
6.914
7.957
9.395
9.639
10.12
19.44
TOTAL 1
AREA
1888
10554
218988
718
1351
1416
£58
684
327233
2364
sea
856975
FILE
METHOD
CONC
0
Q882
HftME
£8.£424 CS2
0.1353 HHA
79.3954 STYREHE
8. ££69 CUME11E
188
ro
Ul
6
N>
o
to
XI
-------
5.25
6.233
6.9
7.952
o ? o a.
4.019
CHROMATGGRAM 1 MEMORIZED
CR5B1 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT HO 99
PKNO
TIME
AREA MK I UNO
1
£
3
4
5
6
-»
/
8
9
10
11
1.59
3.01 5
4.019
5. £5 "•'•;.-
6.233
6.9
7.952
9. 389
9.634
19.108
10.437
1090
18648
.. 215086
738
1413
1481
263
684
378962
£952
444
FILE
METHOD
CONC
0
8002
1
£
NAME
TOTAL
1113760
19.5393 CSS
6. 1348 Mt1A
80.Q161 STYRENE
0.E688 CIJMEI1E
10G
-------
61:35:4897/85/30
4.BE
6.246
6.914
9.64
CHROtlflTOGRflM 1 MEMORIZED
LASCO TUBES
CR581 CHRGMATOPAC
HANNEL MO 1
AMPLE NO 8
EPORT NO 100
KMO TIME
1 4.82
£ 6. £46
3 6.914
4 9.64
AREA MK
£10614
1237
489
3347
I DM0
4
1
o
1
FILE
METHOD
CONC
98.
8.
1.
0
BBSS
NAME
£113 CSS
££79 MttA
5608 STYRE
TOTAL
E15687
IO
KJ
CO
.6
IO
o
CO
^1
6
NJ
100
-------
6.£33
6.9'
9.634
4.016
CHROMATOGRAM 1 MEMORIZED
CR501 CHROMAT'QPAC
CMAHHEL HO 1
SAMPLE HO 8
REPORT NO 101
FILE
METHOD
0
(D802
KNO
1
f,
c
•-*
o
4
TIME
4.816
6. £33
6.9
9.634
AREA
£19458
132S
514
3550
MK I UNO
TOTAL
224844
CONE NAME
93. 1-81-8 CS£
9.2293 UNA
1.5884 STYREHE
100
-------
4.02
6.246
i ^ fi ft
. b o o
CHROflATOGRAd 1 MEHORIZED
CR5B1 CHROI1ATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 102
PKNO
1
£
3
TIME
4.02
6.246
TOTAL
FILE
METHOD
O
Q002
AREA UK IDM0
4
216309
1229
5Q3
212041
1
COHC HAME
99.7613 CS2
9.2387 STYREHE
100
-------
32:35:3397/05/30
4.Q22
6.243
9.642
CHROMATOGRHM 1 MEMORIZED
CR5Q1 CHROtlflTOPAC
CHANNEL MO 1
SAMPLE NO 0
REPORT HO 103
LASCO TUBES
PKNQ
TIME
AREA
IDHO
FILE
METHOD
COMC
0
0002
SJ
CJ
6
8
U)
HA HE
1
£
3
4.D22
6.248
9.642
TOTAL
215489
1278
591
217267
99.7682 CS2
0.2318 STYRENE
1Q9
-------
4.01?
5. £57
6.24
9.625
C
HROMATOGRAM 1 MEMORIZED
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 13
REPORT HO 104
KMO
TIME
TOTAL
FILE
METHOD
AREA
1
2
3
4
4.817
5. £5?
6. £4
9.625
222685
34?
1365
653
IDNO
4
1
CONC NAME
99.7876 CS2
££5049
. 0.29S4 STYRENE
— _ .i:_ — — —
100
-------
1 * i/n i v/ i
4.019
5. £61
6.£46
9.641
CHROMATOGRAM
1 MEMORIZED
CR5Q1 CHROMATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT NO 185
PKHO
3
4
TIME
4.819
5. £61
6.246
9.641
TOTAL
AREA MK IDHO
£18557 i
314
1233
FILE
METHOD
COMC
0
8902
NAME
to
to
u>
6
£1266£'
9.£645 STYREHE
100
-------
814
5.£61
•6.244
6.9
' 4,019
CHROtlflTOGRAII 1 MEMORIZED
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
c
3
4
5
6 •
7' '
8
CHROttATOPAC
NO 1
HO a
NO 106
TII1E
1.539
3.014
4.019
5. £61
6. £44
6.9
9.637
10.108
AREA UK
874
9385
229773
571
1373
682
£87£15
611
JBNO
4
"C*
1
f",
c
FILE
METHOD
CONC
NAME
51.4381 CS£
0.1404 Mflft
48. £792 STYRENE
0.14E4 CUMEHE
TOTAL
441384
100
-------
1
CHROtlflT
CR5D1
CHAHHEL
SAMPLE
REPORT
PKHO
-i
•-i
l_
•"»
•j
4
•::. 5
V. 6
/
8
i . 0 0 4
- 3,'QIE
—— —
5.261
6.244
6. 9
i8."ff'r
8GRAM 1
CHROI1ATOPAC
HO l
HO O
HO 187
TlrtE
1.584
3 .812
4.817
5.261
6.244
6.9 ,:
9.636
18.116
4 .017
4
MEMORIZED
FILE 8
METHOD 8Q02
AREA MK I DM0 COHC NAME
835
8989
213403 4 52.2967 CS2
541
1294
557 3 Q. 1366 MM A
193557 1 47.4333 STYRE
545 2 8.1334 CUME11
I
o.
t
TOTAL
419728
108
-------
04:15:4397/05/39
LASCO TUBES
3.Q26
5.252
6.237
4.013
i ij . i 1 Q
CHROMATOGRAfl
1 MEMORIZED
CR5G1 CHRQHATOPAC
CHANNEL HO 1
SAMPLE HO 9
REPORT HO 108
PKHD
TIME
AREA UK IDHO
FILE
METHOD
CONC
0
6002
HA HE
4
5
6
7
8
9
4.013
5.252
6.237
6.9
9.63S
10.1.16
10.518
£17123
443
1354
939936
1397969
1753181
723
1
2
4.5157 CS2
19.5486 MMA
39.4735 STYREHE
36.4622 CUMEI1E
1Q.325
680
TOTAL
4811701
100
-------
J4:35:4597/85/39
4.G16
5.256
6.241
LASCO TUBES
GtlkM.
CHROHATOGRAM 1 MEMORIZED
CR5G1 CHROMA TOP AC
CHAM MEL HO 1
SAMPLE HO 8
REPORT MO 109
KMO
1
c
3
4
5
6
7
TIME
'". ' 4.016
, 5.256
^ 6.241
6.905
9.634
10. 114
10.831
AREA
216267
444
1356
.935258
1885682
1740868
649
TOTAL
f ILL
METHOD
0
0982
CONC
NAME
4.5262 CSS
19.5739 I1HA -.
39.4653 STYREHE
36.4345 CUMEME
4780523
100
-------
CR501 CHROMATOPAC
CHANNEL MO £
SAMPLE MO 0
REPORT MO 8£
FILE
METHOD
8002
PKNO
i
TIME
£.5£
£.61£
AREA
15069
5EO£
MK
y
I DM0
1
£
CONC
74.
£5.
3364
6636
TOTAL £G£7£
CHROtlATOGRAM 101 MEMORIZED
MA HE
108
-------
2.519
;R581 CHROttATOPAC
;HANHEL HO 2
SAMPLE HO 8
REPORT NO 83
FILE
METHOD
000S
:'KHO
TIME
AREA
I UNO
CDNC
NAME
2.519
2.61S
TOTAL
•ROHATOGRAn 181
144H7
5811
19438
HEMORIZED
74.£199 METHANE
£5.7301 ETHANE
108
-------
£9:31:18
CR501 CHROI1ATOPAC
CHANNEL NO £
SAMPLE HO 8
REPORT HO 84
LASCO BAG
FILE
HETHQD
£.519
ro
KJ
OJ
6
*KNO
1
. £
TIME
£.519
e.sie
TOTAL
AREA t1K IBNO
14515
508? V
1954£
CONC
168
NAME
74. £75 METHANE
£5.725 ETHANE
-------
*
C . O I -J
CR561 CHRQHATQPAC
CHAHNEL NO £
SAMPLE NO 8
REPORT HO 81
2.52
FILE
METHOD
Q
S0BE
\
'1C HO
TItlE
TOTAL
AREA UK 1DHO
1
2
3
2.52
2.61
2.815
13126
1876
587
1 !
*i*
V
14789
COMC
NAME
98.4257 METHANE
7.5742 ETHANE
100
CHROHflTQGRAM 181 MEHORIZED
-------
CR5Q1 CHROIIATOPftC
CHANNEL NO £
SAMPLE NO 8
REPORT NO 88
KHO
1
£
TIME
a.5£
£.61
AREA MK IDHO
FILE
METHOD
CONC
Q
8882
HAME
12497
1885 V
92.5592 METHANE
7.4488 ETHANE
£.815
TOTAL
CHROMATOGRAh 101
547
14848
MEMORIZED
188
-------
2.815
2.52
CR5Q1 CHROHATOPAC
CHANNEL NO £
SAMPLE HO 0
REPORT HO 78
FILE
METHOD
Crj
PKHO
'I HE
TOTAL
AREA MK IDHO
COHC
NAhE
1
£
3
2.
2.
2.
5
6
8
2
1
1
2
5
739Q8
3360
791
1
V 2
1.1
95.6518
4.3482
METHANE
ETHANE
CJ
s
o
CJ
ro-
78859
10Q
-------
2.517
CR5EU CHROttftTOPftC
CHANNEL MO £
SAMPLE NO 8
REPORT NO 77
PKNO
TIME
2,517
£.688
2.814
AREA MK . IDHO
14617 1
1196 V £
£64
FILE
METHOD
CONC
988S
92.4346
7.5654
NAME
I1ETHANE
ETHANE
TOTAL
16077
100
-------
CR581
CHANNEL
SAMPLE
REPORT
PKMO
1
£
3
i
h
a.sa*
V i.
CHROtlftTOPAC
HO
HO
NO
T
2.
£.
2.
£
0
74
IHE
52
61
888
AREA HK
18758
153£ V
336 V
FILE 9
METHOD eeee
I UNO CONC NAHE
1 92.4514 METHANE
£ 7.5486 ETHANE
1013-2.
:.52
TOTAL
28626
188
-------
37/85/29 18:38:28
LASCQ BAG SAMPLES
2.814
2.518
H CHROMATOPAC
CHAMMEL HO £
SAMPLE NO 9
REPORT HO 72
PKNO
TIME
AREA MK IDNO
1
£
3
£.518
2.611
£.814
98948
4283
944
FILE
METHOD
CONC
95
Q
•00 02
NAME
5824 METHANE
4176 ETHANE
TOTAL
96895
1 1:1 fi
-------
.814
a.513
CR581 CHROHATQPAC
CHANNEL HO 2
SAMPLE NO 8
REPORT HO ?B
FILE
METHOD
PKNO
1
£
3
TIME
2.518
S.611
2.814
AREA HK I UNO
91663
4251
95?
COMC
NAME
95.5676 METHANE
4.4324 ETHANE
TOTAL
96872
180
-------
IHROnftTQGRflfl 101 MEMORIZED
/95/£9 17:03:42
LASCO BAG SAMPLES
£.514
CR5D1 CHROMATOPAC
CHANNEL HO £
SAMPLE NO Q
REPORT NO 65
FILE
METHOD
OOB£
t»'
KNO
1
£
T
£.
.r,
c .
I ME
514
684
AREA
19813
1557
MK
V
I DM0
1
£
COMC
92.
7.
/
£
1
Ti
D
33
67
NAME
METHANE
ETHANE
TOTAL
<-. 1 '•••^ r\
C. 1 J f U
100
-------
CHROHATQGRAI1 191 MEMORIZED
87/05/29 16:59:24
LASCO BAG SAMPLES
10
2.51
CR501 CHROHATOPAC
CHANNEL NO 2
SAMPLE NO Q
REPORT NO 64
PKNO
TIME
TOTAL
AREA UK IDNO
FILE
METHOD
COHC
9
8802
NAME
i
2
3
2.
'£.
£.
519
689
814
199QQ
1621 V
£18
1
*».
c
92.
7 .
4692
5398
108
-------
181 MEMORIZED
16:53:IB
F^- £.813
CR581 CHROHATOPAC
CHANNEL NO £
SAMPLE NO 8
REPORT NO 63
LASCO B'AG SAMPLES
FILE
METHOD
2.517
PKHO
1
TIME
2.517
AREA
88318
UK
IDNO
1
CONC NAME
95.5298 METHANE
£.61
£.813
3758
897
4.470e ETHANE
TOTAL
84973
100
-------
L'HROHATOGRAM 1G1
37/85/29
2.8M
MEMORIZED
16:36:09
LASCO BAG SAMPLES
2.513
CR501 CHROMATOPAC
CHANNEL HO 2
SAMPLE NO B
REPORT HO 61
PKMO
1
TIME
£.518
E.6S9
£.314
AREA UK I DUO
FILE
METHOD
COHC
9
0662
NAME
18966
1550 V
31S V
92.4231 METHANE
7.5769 ETHANE
CJ
6
ro
--4
6
KJ
TOTAL
£8774
188
-------
;HROMATOGRAM 101 MEMORIZED
'/65/£9 16:44:04
^— £.813
CR501 CHROI1ATOFAC
CHftHHEL HO 2
SAMPLE HO 6
REPORT HO 68
LASCO BAG SAMPLES
FILE
METHOD
9
6662
9-13-1
2.517
©
PKNO
TIME
2.517
£.61
£.813
AREA MK IDHO
37617
4077 V
967
1
1-1
COHC
NAME
95.5534 METHANE
4.4466 ETHANE
TOTAL
92661
1G9
-------
:.HROf1ATOGRAH IQl MEMORIZED
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
2
3
^'•/UJ/'ciy lb! 05:^1-' LASCO KAb oAMKLL'o
f- 2 . S l1^ " A ;
CHROMATOPAC
HO £ FILE 9
NO 8 METHOD 6082
HO 69
TIME AREA UK IDHO COHC NAME
2.519 13933 1 92.3664 METHANE
2.61 1565 V £ 7.6335 ETHANE
'2.815 336 V
2.519
TOTAL
2883;
,:, 198
-------
QGRAN 101 MEMORIZED
37/95/29 16: 90.: 44 . LASCO BAG SAMPLES
9-
f £.313 l"bl
CHRQMATOPAC
MO 2 FILE 9
MCI 6 METHOD. 6682
CR501
CHAMI1
SAMPLE MO
REPORT NO 59
2.517
PKNO
TIME
£.517
£. b 1
£.813
AREA MK IDM0
89787
3758 V
941 V
COHC
NAME
95.5546 METHANE
4.4454 ETHANE
TOTAL
85486
106
-------
w««nn iQi ntnuRIZED
97/65/29 15:54:59
i_ £.814 l-*t'li
CR561 CHROttATOPAC
CHANNEL HO £
SAMPLE HO 0
REPORT HO 58
PKNO TIME AREA MK I UNO
1 2.518 88294 1
£ £.611 3?£5 V £
3 £.814 925 V
LASCO BAG SAMPLES
^.
FILE 9
METHOD QQ8£
COHC MAI1E
95.5665 METHANE
4.4335 ETHANE
2.518
o
CO
o
TOTAL
4944
189
K3
KJ
U
6.
K)
O
CO
x|
6
NJ
-------
£.513
2.517
CR501 CHROI1ATOPAC
CHANNEL HO £
SAMPLE HO 0
REPORT HO 50
PKNO TIHE
1 £.517
£ £.61
3 2.813
AREA UK
38406
4086 V
942
I DUO
1
£
FILE
METHOD
COMC
9
8882
NAME
TOTAL
93433
95.5327 METHANE
4.4173 ETHANE
100
-------
13:20:28
£.812
LASCO BAG SAMPLES
L. . O U 7
2.516
CR501 CHROtlATOPAC
CHANNEL HO £
SAMPLE HO 8
FILE
METHOD
9
8Q0S
U)
6
REPORT NO 49
PKNO TIME
1 2.516
2 £.669
3 2.312
AREA MK IDM0
87352 1
4G35 V 2
COMC
HAI1E
95.5348 METHANE
4.4152 ETHANE
TOTAL
923,14
iee
e.
-------
CHROMATOGRAM 101 MEMORIZED
<"'«'« 10:44:15
CR5B1 CHROMATOPAC
CHANNEL HO £
SAMPLE NO 6
REPORT HO 41
PKNO
1
£
3
TIME
£.517
£.61
2.813
UK
64000
304S V
74 £ V
LASCO BAG SAMPLES
TILE
METHOD
CONC
£.517
HAME
95.4621 METHANE
4.5379 ETHANE
TOTAL
67784
100
-------
CHROI1ATOGRAM 101 MEMORIZED
10:33:17
•;, o i "-i
L. i O 1 C-
LASCO BAG SAMPLES
2.518
i
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE HO Q
REPORT HO 40
FILE
METHOD
Q
D0DE
PKNO
1
£
TIME
£.518
2.61
2. S13
AREA MK IDNO
3138
765
£
CDNC
NAME
95.4807 METHANE
4.5193 ETHANE
TOTAL
70265
108
-------
:HROMATOGRAH 101
37/Q5/29
HEHORI2ED
10: £8: 48
LASCO BAG SAMPLES
c. s i;
£.517
CR501 CHROtlATOPAC
CHAMMEL HO £
SAMPLE MO 0
REPORT HO 39
FILE
METHOD
9
GBBE
KMQ
TIME:
AREA MK IDHO
CONC
NAME
2.517
£.688
£.812
TOTAL
16669
1341
185Q
>«•»««•
19860
£
92.5534 METHANE
7.-4466 ETHANE
190
o
IO
to
-------
10:23:14
w . uuv.., o 1 ,.,
^^ C.O1C
LASCO BftG SAMPLES
1
-------
2.507
CR5Q1 CHROMATOPAC
CHflHMEL HO £
SAMPLE NO 8
REPORT HO 31
FILE
METHOD
9
000S
PKMO
1
c
TIME
2.5Q7
2.599
AREA
14619
5067
MK
V
I DM0
1
2
cone
74.
25.
259
741
NAME
TOTAL 19666
CHROMATOGRAM 101 MEMORIZED
100
-------
!
CR561
CHANNEL
SAMPLE
REPORT
f'KNO
1
£
1
CHROHflTOPAC
NO £
NO 8
HO 3£
TIME AREA MK
£.588 149££
£.601 5166 V
C « v U 1
FILE 9
METHOD 8
IDNO COMC
1 74. £841
' £ £5.7159
80E
NAME
HETHANE
ETHANE
£.588
TOTAL
o
£0087
168
K9
OJ
-------
• n r,. u 11 u i u u n M 11 i ij i
37/85/E0
1 1 1. n u K i £ L 11
16:55:23
LASCO BAG SAMPLES
810
£.495
CR501 CHROMATOPAC
CHANNEL HO £
SAMPLE NO 0
REPORT HO £68
PKMO
TINE
AREA UK IDHO
FILE
METHOD
COHC
9
B00£
NAME
1 2.495
2 2.536
3 2.733
TOTAL
HROMATOGRAM 101
' 'i
37/85/28
21062
11 20 V
506
22688
MEMORIZED
17:00:33
;C " V '
1 94.9529 METHANE
£ 5.0471 ETHANE
100
LASCO BAG SAMPLES
2.494
CR5B1 CHROMATOPAC
CHANNEL MO £
SAMPLE NO 0
REPORT NO £69
?KNO
1
TIME
£.494
AREA MK IDNO
£0324 1
TILE
METHOD
B00£
COHC HAME
94.9189 METHANE
2
3
£.585
2.737
1088
512
5.0811 ETHAME
TflTCil
21923
196
-------
CHRQMftTQGRftn 161
37/85/20
MEMORIZED
16:44:55
LASCO EAG SAMPLES
2.493
CR561 CHROMATOPAC
CHANNEL MO 2
SAMPLE HO B
REPORT MO £66
FILE
METHOD
9
0002
PKHO
1
£
3
TIME
2.493
2.585
AREA UK I DUO
112319 1
456? V 2
1057
COMC
NAME
96.0931 METHANE
3.9969 ETHANE
TOTAL
:HROI1ATOGRA11 101
97/05/20
117942
MEMORIZED
16:49:51
100
LASCO BAG SAMPLES
e9
a
•••)
eft
2.494
CR581 CHROI1ATOPAC
CHAMMEL NO 2
SAMPLE NO 0
REPORT NO 267
PKNO
TIME
AREA MK IDNO
FILE
METHOD
CONG
1
2
3
2.494
2.586
2.787
TOTAL
114910
4611
1881
128603
V
V
1
2
9
OD02
M
CJ
6
OJ
V4
NAME
96. 1413 METHANE
3.8582 ETHANE
186
-------
:HROHATi
1
CR5Q1
CHANNEL
SAMPLE
REPORT
PKNO
1
£
•t
•J
jGRfill 131 MEMORIZED
47/05/£0 16:31: 48
;. — 0. 47£
:HRQMATOPAC
NO £
10 9
•10 £64
T.I HE
0.472
£.494
£.596
TOTAL
CHROHATOGRAI1 101
87/05/20
CR581
CHANNEL
SAMPLE
REPORT
PKNO
1
2
3
L=
CHROMflTOPAC
NO £
HO 9
NO £65
TIME
0.937
2.495
2.587 ,
AREA MK
6116
63187
5745 ''f
75048
MEMORIZED
16:36:47
U.937
AREA MK
6817
64599
5868 V
LASCO BAG SAMPLES ^
u. . •J'.'O
FILE 9
METHQ.D 8BO£
ID HO COHC NAME
1 91.6656 METHANE
£ 8.3344 ETHANE
100
LASCO BAG SAMPLES
iL •
-------
97/85/c
IS:52357
:.7S6
CR561 CHROMATOPAC
CHANNEL NO £
SftllPLE NO 9
REPORT NO £74
LflSCO BAG SAMPLES
'0
2.491
CJ
6
8
u
6
NJ
PKNO
TIME
1
£
3
2.491
£.584
• 2.786
75045
3888
726
AREA HK IDHO
FILE
METHOD
CONC
NAME
TOTAL
'8853
96.848 METHANE
3.95£ ETHANE
108
-------
CHROMAT
34:55:1997/05/30
1.587
.3.023
. ==••••••
6. £43
6.916
OGRAM 1
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE NO 0
REPORT NO 110
PKMO TIME
1 1.587
£ 3.023
3 4.623
4 6. £48
5 6.916
6 9.639
7
10.121
TOTAL
4.023
MEMORIZED
AREA MK
330
3106
214342
1273
459
85960
368
3FI5837
LASCO TUBES
FILE 0
METHOD 0002
I UNO CONC NAME
4 71. 1795 CS2
3 0. 15£4 MMA
1 £8.546 STYRENE
2 9.1221 CUHEHE
i no
-------
1.585
3. G1 9
6.246
6.914
4.92
CHRQHATOGRAH
1
MEMORIZED
CHR0MATOPAC
CHANNEL NO 1
C'HnrLL
REPORT
PKNO
1
••^
c
4
6
7
NO 0
NO in
TIME
1.535
3.019
4.02
6.246
6.914
9.638
10.12
AREA
329
3173
221442
1316
4S5
99963
422
UK
TOTAL
313129
FILE
METHOD
CONC
0
GG02
NAME
70.6779 CS2
0-1547 MMA
0328
TVRENE
0.1245 CUMEME
100
-------
J t W •
:' j •
'
X*-!
1.
•-(
'-' •
5.
6.
6.
: 1 9 9 7 / n 5 / ? o L A c; C
585
816
^—~ 1 n 1 ^
^^^ 4 . U i J
£55
24
907
16. ITS"
CHROMATQGRAM 1 MEMORIZED
CR5B1 CHROI1ATOPAC
CHANNEL HO 1
SAMPLE NO 0
REPORT HO 112
PKNO
1
2
3
• $/
5:
6
7
8
TIME
1.535
3.01 6
4.015
•«• 5,255
6.24
6.907
9.633
18. 115
AREA
476
3418
£23144
454
1382
1892
197234
514
FILE
METHOD
COMC
0
8002
NAME
TOTAL
427787
=; •:• o 7 o 7 r- o
•j c.. o i- ? .• 0 v»
8.2589 MMA-
46.7396 STYRENE
0.1218 CUMEME
180
-------
i . J b 8
3. 621
5.261'
6.247
6.914
10. iW1
CHROHATOGRAI1 1
CR501 CHROI1ATOPAC
CHAHMEL HO 1
SAMPLE- HO 6
REPORT NO 113
PKNO TIME
1 1.5:38
£ 3 . Q E 1
3 4. 821
4 5.261
5 6.247
6 6.914
7 9.633
8
10.108
TOTAL
4.021
MEMORIZED
AREA MK
476
3350
£17081
436
130S
1036
184270
475
408432
FILE 0
METHOD BBB2
I DM0 COMC NAME
4 53.SS4S CS2
3 0.2572 MMA
1 45.7491 STYRENE
2 0. 1178 CUHEHE
100
to
w
ui
-------
CHROMAT
16:35:2397/05/30
1.587
—3.01
5. £5
6.246
6.91 2
OGRAM 1
CR501 CHROMATOPAC
CHANNEL NO 1
SAMPLE NO 8
REPORT HO 115
PKNO TIME
1 1.537
£ 3.01
3 4.821
4 5. £5
5 6.246
fa 6.912
7 9.636
8
10.116
TOTAL
4.021
MEMORIZED
AREA MK
370
£6457
215672
821
1386
1988
215052
506
462673
LASCO TUBES
i
,
.
FILE : 0
METHOD 8882
I UNO CONC ' NAME
v , .4 49.7333 CS2
3 0.4588 I1MA
1 49.6407 STYRE
£ 0.1167 CUMEI-
18B
to
ro
Id
6
to
o
to
vj
6
ro
-------
1.575
• 3.014
r =••—
H!3
•j • ^ j
6. £45
6.912
o 003 , .
HD.10-8'""'
CHROdATQGRAII 1
CR501
CHAHNEL
SAMPLE
REPORT
PKMO
1
£
O
•j
4
5
b
7
n
C-
9
10
CHROHATOPAC
HO 1
HO 8
HO 116
TIME
1.575
3.D14
4.02
4.858
5.25
6.245
6.912
9.383
9.636
10.108
TOTAL
4,02
V
MEMORIZED
AREA 11 K
694
6939
£20642
528
692
1489
1135
36B
522127
HOE
755107
FILE 0
METHOD 0002
I UNO COHC NAME
4 29.6042 CSS
3 9.1522 MNA
1 70.6554 STYRENE
£ D.1881 CUNEME
106
-------
CHROMAT
CR501
CHANNEL
SAMPLE
REPORT
f'KNO
1
o
.3 .
4
5
6
7
8
9
10
37:15:3497/85/38 LASCO TUBES M
1.587
• 3.815
* J * C U i
6. £33
6.9
0 -511
OGRAM 1
CHROtlATOP
HO 1
NO 8
NO 11?
TIME
1.587
3.015
4.617
4.866
5.257
6.233
6.9
9.391
9.636
10.119
TOTAL
— 4.017 ' :
i
E
MEMORIZED j
AC
. FILE : 0
METHOD 0002
AREA UK I UNO CONC NAME
669
5802
215533 4 29.9671 CS2
. 507
661
14£6
1890 3 0.1516 HMA
340
581291 1 69.698 STYRENE
1319 2 S.1834 CUHEHE
728638 100
r-i.
o
•J1
K3
N»
1
CJ
-------
CHROI1AT
CR5G1
CHANNEL
SAHPLE
REPORT
PKNCl
1
J-i
L.
'•l
\j
4
5
6
7
8
1.588
=-—:•:. 009
, 5.256
6.233
6.9
10.115'"-"-
OGRAM 1
CHROMATOPPC
NO 1
HO 0
NO 114
TIME:
1.583
3. OG9
4.019
5. £56
6. £33
6.9
9.632
10. 115
4^1 j p.
.019
MEMORIZED
AREfi f1K
1921
396£3
£34821
950
1498
£279
£48058
653
FILE 0
METHOD 0002
IDNO COHC NAME:
4 43.3359 CS2
':. '
3 G. 4692 MM A
1 51.9^86 STYRE
£ O. 1343 CUMEM
TOTAL
519903
18.Q
-------
J7:35:3697/G5/30
1.5S6
• 3.Q.11
LASCO TUBES
4.92
5.25
6.243
6.9
ie.it
CHROHATOGRAH 1 MEMORIZED
CR581 CHROtlATOPAC
CHANNEL NO 1
SAMPLE HO 0
REPORT HO 118
PKNO
TIME
TOTAL
AREA MK IDNO
FILE
METHOD
CONG
O
ooos
532985
NAME
1
£
5
6
7
8
Q
1.
3.
5.
6.
6.
9.
9.
16.
536
Oil
25
243
9
337
631
111
1072 ,
1674.©-;-
,242563:'
1034
1729
743
252
317929
924
4
'i
w'
1
2
43.
0.
56.
0.
1435
1321
5551
1643
CS2
11 fl A
STYRENE
CUMEME
180
-------
|B7: 55: 3497/85/38
LASCO TUBES
1
1.585
- 3.01
r r • '
5.25?
6.233
6.9
10."iWJ "
CHROMATOGRAM 1
CR501
CHANNEL
SAMPLE
REPORT
PKNQ
1
c
3
4
5
6
7.
8
9
CHROMATOPAC
HO 1
NO 8
HO 119
TIME
1.585
3.81
4.888
5.257'
6.233
6.9
9,39£
9.635
18.188
TOTAL
4.888
MEMORIZED
FILE 8
METHOD 0882
AREA MK IDHO CONC NAME
881
13692
213426 4 45.575 CSS
•*25«, ,
1394
594 3 0.1 £69 tlHfl
283
£53564 1 54.146 STYRE
712 2 0.1521 CUMEt-
485298 188
KJ
ro
©
-------
4 . Q 1 8
5.25
6.241
7.942
•a
CHROMATOGRAM 1 MEMORIZED
CR591 CHROMATOFAC
CHANNEL NO
SAMPLE NO
REPORT NO
PKNO
1
8
129
TIME
AREA UK IDM0
FILE
METHOD
COHC
0
0992
NAME
4
5
6
7
8
9
10
11
12
13
14
15
16
1.375
1.586
1.833
£.148
3.Q32
4.013
5. £5
6. £41
7.942
9.275
9.386
9.63£
19.112
10.417
10.583
18.7
£63
1923
335
£77
743
£ 1 8 1 1 £
832
1686
£74
£51
1336
1552161
4812
1613
1877
245
12.2874 CS£
1
£
87.4415 STYRENE
0.2711 CUMEME
TOTAL
1785912
100
-------
J8:35:4597/Q5/3Q
11..
2:
LASCO TUBES
3.017
-••
5. £57
6.233
7.948
3 ggfi
4.813
en
CO
flliiii
CHROHATOGRAH 1 MEMORIZED
CR501 CHROMATOPAC
CHAMMEL HO 1
SAMPLE MO 0
REPORT MO 1E1
K)
K]
U
6
ro
O
F'KNO
4
5
S
9
ID
11
IE
13
TIME
AREA flK IDM0
1.354
1.584
1.89
£.146
3.017
4.813
5.257
6. £38
7.948
9. £75
9.3S6
9.63£
10. 115
£49
1912
381
£76
722
£14245
813
1575
27Q
319
1473
153£5£6
47Q6
FILE
METHOD
COMC
0
G00£
NAHE
1*".
c .
, ,
o c c
87.4991
0.2687
STYREHE
CUMEI1E
14
15
16
17
10.4£9
10.597
10.708
18.833
1566
1141
322
712
I I
V
V
V
TOTAL
1763207
100
-------
.816
5.256
6.233
•J . J U -J
CHROHATDGRAtt 1 MEMORIZED
CR501 CHROHATOPAC
CHANNEL HO 1
SAMPLE HO 0
REPORT HO 1££
FILE
METHOD
0
0062
PKNO
1
TIME
AREA MK IDNO
4.016
5.256
6.233
6.9Q5
9.638
10.122
214380
426
1332
916432
1874301
1736764
COHC HAHE
4.5251 CS2
< O "' c. 1
i 7 . j J 1 i
MMA .
39.5773 STYRENE
36.5464 CUtlEME
•.3
•O
10.524
10.S33
TOTAL
£29
678
4738464
106
-------
' [i t- S
6
KJ
o
CJ
>j
6
ro
.322
6.246
i 10.53;
::HROt1ftTOGRAM
i. ' J i i i
1 MEMORIZED
CR501 CHROHATQPAC
CHflMMEL HO 1
SAMPLE HO 0
REPORT HO 1£3
FILE
METHOD
6
eeee
KMO
TIME
AREA MK IDHO
COHC
HA ME
1
2
•-i
4
5
c-
.022
.261
.246
•j
1
3
1
1
X
4
3
46
37
23
4.6152 CSS
4
5
6
7
6.909
9.637
10. 119
10.837
TOTAL
906916
1319724
1678605 V
664
4629S19
19.6371
39.4817
36.3461
100
STYREHE
CUMEME
-------
1111\ U 11 M I U U K HII 1 tl 1
37/65/26
nt.nuKiiit.iJ
£1:14:12
LASCO BAG SAMPLES
CR5D1 CHROMATOPAC
CHANNEL HO £
SAMPLE HO 6
REPORT HO £85
PKNO
TII1E
AREA MK IDHO
FILE
nETHOD
COHC
9
0982
NAME
£
2.492
£.585
2.736
71308
£897
£4778
V
V
1
£
96.0956
3.9043
TOTAL 93983
CHROMATOGRAM 191 MEMORIZED
21:20:09
100
LASCO BAG SAMPLES
o
vO
2.491
2.735
CR561 CHROMATOPAC
CHANNEL HO £
SAMPLE MO 0
REPORT MO £86
PKHO
TII1E
AREA MK IDHO
FILE
METHOD
COHC
9
Q082
HAME
KJ
CJ
6
10
1
s
3
2.
2.
2.
491
584
735
63136
£76£
19690
V
1
£
96.
3.
1872
89£8
TOTAL
101
90543
100
-------
CR581 CHROHATOPAC
CHANNEL HO £
SAMPLE NO 8
REPORT NO £87
PKNO
c.
3
TIME
£.492
£.584
2.786
AREA t1K IDNO
FILE
METHOD
COHC
9
G00£
NAME
17249
939 V
18279 V
TOTAL 36467
CHRQHATOGRAH 1Q1 MEMORIZED
?7'/Fi5/£0 £1:30: 17
94.8372 METHANE
5.16E-8 ETHANE
108
LASCO BAG SAMPLES
CR501 CHROMATOPAC
CHANNEL HO £
SAMPLE NO 0
REPORT NO 288
PKNO
1
£
TIME
2.491
£.583
2.785
AREA MK IDNO
FILE
METHOD
CONC
9
9902
NAME
16656
885 V
17661
1
£
94.9553 METHANE
5.8447 ETHANE
TOTAL
352Q2
100
-------
F
2.51
CR5B1 CHROI1ATOPAC
CHANNEL NO £
SAMPLE MO 8
REPORT HO 91
PKMO
TIME
1
£
3
2.51
2.681
2.885
19854
1246
371
AREA MK IDM0
1
TOTAL £1478
CHROMATOGRAM 101 MEMORIZED
37/Q5/23 13:59:97
FILE
METHOD
COMC
9
6002
NAME
94.0962 METHANE
5.9838 ETHAME
LASCO BAG SAMPLES
:.503
CR561 CHROMATOPAC
CHANNEL MO £
SAMPLE MO 6
REPORT HO 92
PKNO
£
TIME
2.503
2.593
2.797
AREA MK I DUO
20881
1248
378
FILE
METHOD
CONG
2
9
00B£
NAME
94. 1235 METHANE
5.8715 ETHANE
TOTAL
21627
100
-------
1
»?/65/£3 13:48:57 LASCO BAG • SAMPLES J
— 2.8941-'01"1
CR501 CHROMATOPAC
CHANNEL HO £ FILE 9
SAMPLE NO 0 METHOD 8Q0S
REPORT HO 39
PKNO
1
£
3
CHROMAT
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
£
3
TIME AREA MK IDNO CONC NAME !
2.503 5£973 1 95.8771 METHANE
£.601 ££78 V £ 4.1 ££9 ETHANE
2.804 91£ V
TOTAL 5616£ . 100
OGRAM 161 MEMORIZED
37/65/E3 13:49:34 LASCO BAG SAMPLES
CHROHATOPAC
. NO £ FILE 3
NO 0 METHOD DB02
HO 90
TIME AREA MK IDNO CONC NAME
£.503 54684 1 95.3£££ METHANE
£.601 1Q76 V £ 4. 1776 ETHANE
£.804 4£8 V
£.588
oo
2.503
N>
ro
TOTAL £6138
CHROMATOGRAM 181 MEMORIZED
-------
37/85/23
MEMORIZED
i£:£9:01
LASCO BAG SAMPLES
00
2.498
CR501 CHROMATOPAC
CHfiHHEL HO £
SAMPLE NO Q
REPORT NO 85
PKNO
TIME
AREA UK IDM0
TILE
METHOD
CONC
9
0002
NAME
en
£.498
£.588
£.793
TOTAL
CHRQMATOGRAII 191
13808
930
181
14919
MEMORIZED
12:33:38
93.6399 METHANE
6.3101 ETHANE
100
LASCO BAG SAMPLES
to
KJ
OJ
6
KJ
o
u>
NJ
6
KJ
\0~\\-z.
2.499
CR501 CHROHflTOPftC
CHANNEL HO £
SAMPLE NO 0
REPORT NO 86
FKNO
TIME
AREA UK IDNO
1
E
FILE
METHOD
CONC
1
£
3
2.499
£.589
2.793
TOTAL
14293
960
187
15445
V
V
NAME
93.7092 METHANE
6.£907 ETHANE
100
-------
CR501
CHANNEL
SAMPLE
REPORT
PKNO
1
C
•".
-------
i •-• u ix n 1 1
37/65/23
11:43:31
LASCO BAG SAMPLES
IffrlH
2.495
V4
6
10
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 8
REPORT NO 30
KMO
TIME
AREA MK I UNO
1 2.495
£ £.585
3 £.738
TOTAL
HROMATOGRAM 1G1
37/05/23
21969
1485 V
345 V
£3799
MEMORIZED
11:47:51
FILE
METHOD
COHC
9
00B2
NAME
£.7?"
93.6674 METHANE
6.3326 ETHANE
100
LASCO BAG SAMPLES
J4-//-J
2.497
CR5Q1 CHROMATOPAC
CHAMMEL NO £
SAMPLE NO 0
REPORT NO 81
PKNO
1
£
3
TIME
£.497
£.587
£.79
TOTAL
AREA MK I UNO
£0647
1409 V
320 V
£2375
FILE
METHOD
COMC
9
OOQ£
NAME
93.6137 METHANE
6.3863 ETHANE
100
-------
,• n i\ u 11 n i i_> u ft m I i o
57/85/£3
n c. n u K a <: t u
11:06:08
£.783
LASCO BAG SAMPLES
2.49
CR5Q1 CHROMATOPAC
CHANNEL HO £
SAMPLE NO 0
REPORT HO 76
FILE
METHOD
9
0902
PKMO
TIME
AREA MK IDHO
COMC
NAME
1
£
3
£.49
£.581
£.733
52339
2329
578
V
V
1
ft
c
95.7402
4.2598
TOTAL
35245
100
::HROMATOGRAM 101 MEMORIZED
3 11:25:46
£.785
LASCO BAG SAMPLES
KJ
IO
Ul
2.491
CS5Q1 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 0
REPORT NO 77
FILE
METHOD
9
0002
PKMO
1
2
TIME
2.491
2.582
2.735
TOTAL
AREA UK
49733
2228 V
562 V
52523
IDHO
1
COMC
95.7118
4.2882
HAME
METHANE
ETHANE
100
-------
* 1.SS3
3.087
i «
- . C C J
6. £ 1 3
997
I 10.7S3
CHRQMATQGRAH 1 MEMORIZED
CR5Q1 CHROHATQPAC
CHANNEL HO 1
SAMPLE HO G
REPORT HO 2
FILE
METHOD
8
0002
'KNO
TIME
AREA MK IDM0
COMC
MAME
1
2
3
4
;<5
•:vjs
7'
3
9
19
1.333
3.807
3.997
C -'I -'I •",
•-' . u C. • j
6.213
6.S73
9.242
9.6
10.03
10.733
2653
105Q
220479 4
5593 .-
343 'v:
737574" 3
1357
1579553 V 1
1454962 V 2
602
5,5222 C32
•"••;
13.4737 iiMA
Q
39.5623 STYREHE
36.4417 CIMEME
TOTAL
4004171
100
-------
S
LJ
X
6
Is)
I
2.43
CR501
CHRQHATQPAC
CHANNEL MO £
S ft n P L E H 0 13
REPORT HO 74
7 i r
FIL
METHOD
?KNO
TINE
AREA MK IDNO
COHC
MA HE
1
£
£.43
£.571
TOTAL
;HROHATOGRAM 101
97/85/23
15638
5838
£1476
MEMORIZED
09:27:33
72.8168 METHANE
£7.1831 ETHANE
108
LASCO EAG SAMPLES
£.43£
CR581 CHROHATOPflC
CHAM MEL NO £
SAMPLE NO Q
REPORT HO 75
FILE
METHOD
9
8082
PKMO
TIME
AREA MK I DUO
CONC
NAME
£
£.48£
£.574
15573
5830
1
£
72.769 METHANE
£7.231 ETHAHE
TOTAL
£1408
100
-5/7
-------
16: 47: i;-'y//1j.1,/c1 y
1
333
3.897
6. £ 1 3
L H * !„ U I U & C. 3
I 18.783
CHROMATQGRAM 1 MEMORIZED
CS501 CHROMATOPAC
CHANNEL NO 1
3AMPLE MO 0
REPORT HO £
FILE
METHOD
6
0002
KNO
1
il
. 3? ";
4
5
6
7
3
9
18
. T
1 .
3.
3,.
5^;
6 .
6 .
9.
9.
10.
10.
I HE
333
007
997
223
£13
373
242
6
03
733
AREA riK IBNO
•- £ tr c-i
C b -J 0
1050
228479 4
5593
343 :•'
737574 3
1357
1579553 V 1
1454962 V 2
602
CQNC NAME
5.5222 CS2
13.4737 MMA
39.5623 STYREME
36.4417 CUMEME
TOTAL
4004171
100
-------
.
/
£9:1697/05/28
5.175
7.736
'.t'lj''
' » V ••' T
LASCO TUBES
3.9'64
o
o
CHRQHATOGRAM 1 MEMORIZED
CR5-Q1 CHROMATQPAC
CHAMMEL HO 1
SAMPLE HO 0
REPORT MO 1
'KNO
TIME
<4REft MK IBMO
FILE
METHOD
COMC
ro
to
CJ
6
N>
O
NAHE
1
2
3
4
5
6
7
8
9
1.879
2.967
3.964
5.175
6.849
7.736
9. '20 3
9.579
10.054
£735
11QS
214354
763S
753935
8903
26076
162369Q
1439575
V
V
TOTAL
4133015
2
52.2386 STYREME
47.7693 CUMEME
100
-------
37/85/22 £1:26:49
LftSEO BAG SAMPLES
£.493
£.793
CR501 CHROHATQPAC
CHANNEL MO £
SAMPLE 110 0
REPORT NO 45
PKMO
TIME
1
£
3 -
£.498
£.59
£.793
59690
£430 V
32181 V
AREA UK IDNO
1
FILE
METHOD
CONC
9
88B2
NAME
£
96.8506 METHANE
3.5494 ETHANE
TOTAL 936£1
CHROHATOGRAH 191 MEtlORIZEH
188
-------
21:00:49
2/79*4*
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 0
REPORT NO 43
LASCO BAG SAMPLES
PKNO
i
TIME
£.499
AREA UK IDhO
11844 1
FILE
METHOD
£.499
9
000e
CONC NAME
93.85£4 METHANE
£
3
£.59
£.794
£86
6.1476 ETHANE
TOTAL
11967
190
-------
37/65/22
•"• 1 • o o«
c. 1 • o c«
LASCO BAG SAMPLES
CR5Q1 CHROMATQPAC
CHANNEL MO £ ,
SAMPLE NO 0
REPORT NO 46
F'KNO
TIME
AREA UK IDHO
FILE
METHOD
CONC
TOTAL 94565
CHROMATOGRAM 101 MEMORIZED
NAME
1
2
3
£.498
£.589
£.791
69892
£4?£ V
31 £01 V
1
£
96.Q984
3.9Q16
198
-------
3riROMATOGRAM 101
57/05/19
MEMORIZED
12:45:00
LASCO BAG SAMPLES
£.791
0PEH9
2.493
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE HO 0
REPORT NO 194
PKHO" '
TIME
AREA .-MK' IDHO
FILE
METHOD
COHC
q
0002
NAME
1
£
3
CHROHAT
CR591
CHANNEL
SAMPLE
£.498
£.59
£.791
TOTAL
OGRAM 1
J7/05/1
•"•
CHROMAT
HO 2
HO O
125902 1 96.0947 METHANE
5117 V £ 3. 9053 ETHANE
1170 V
132189 100
01. MEMORIZED
9 13:i£:5£ LASCO BAG SAMPLES
2.793 l"J3u
OPAC
FILE 9
METHOD 0002
o
on
tfW
M
OJ
6
K)
O
OJ
SJ
6
K)
REPORT HO 195
PKHO
TIME
AREA MK IDNO
CONC
NAME
1
£
3
2.499
£.592
2.793
126723
5169
1170
V
V
1
£
96.
r,
w1 •
0813
9187
TOTAL
133066
106
-------
;HROMATOGRAM 101
57/95/19
MEMORIZED
1 3; 7 ?! c, o
2:
LASCO BAG SAMPLES
2.502
CR5Q1 CHROMATOPAC
CHAHHEL MO 2
SAMPLE NO 0
REPORT NO 196
PKHO
TIME
AREA MK I DM0
1
2
3
2.
2.
2.
502
593
796
18342
1
049
181
V
v
1
2
FILE
METHOD
CQNC
QOG2
HftME
94.5393 METHANE
5.4106 ETHANE
w
''" TOTAL
CHROMATOGRAM 101
57/05/19
19578
MEMORIZED
13:48:02
13Q
LASCO BAG SAMPLES
2.502
CR581 CHRQttATOPAC
CHANNEL HO 2
SAMPLE HO 0
REPORT HO 197
PKHO
TIME
TOTAL
AREA MK IDHO
FILE
METHOD
CONC
9
8002
17910
NAME
1
2
3
2.592
2.593
2.796
16781
962
167
V
V
1
£
94.5774
5.4£25
o
i.
en
-------
CHROMAHiGRAM 131
57/85/19
MEMORIZED
14:07:35
£.795
LASCQ BAG SAMPLES
£.501
CR5D1 CHROMATOPAC
CHANNEL NO £
SAMPLE MO Q
REPORT NO 199
PKNO
1
£
TIME
£.581
£.593
AREA MK IDHO
117354
4805
FILE
METHOD
CONC
q
0062
1
£
NAME
96.0663 METHANE
3.9337 ETHANE
£.795
TOTAL
CHROHATOGRAM 191
37/05/19
1£49
123408
MEMORIZED
14:14:58
100
LASCO BAG SAMPLES
£.796
2.583
CR501 CHROMATOPAC.
CHANNEL NO £
SAMPLE NO D
REPORT NO £06
PKNO
TIME
TOTAL
AREA MK IDNO
FILE
METHOD
CONC
9
OQO£
125404
NAME
1
£
3
2.503
£.595
2.796
119232
4897
1275
'•!
V
1
£
96.0546
3.9454
100
-------
CHRomuoGRftn i-ei
S7/05/19
MEMORIZED
14:££:Q3
LASCO BAG SAMPLES
/85/19
AREA HK I DUO
£2818 1
1261 V £
381 V
£4461
MEMORIZED
14:
£?
£8
CONC
NAME
94.7615 METHANE
5. £385 ETHANE
188
LASCO BAG SAMPLES
!.586
CR5B1 CHROMATOPAC
CHAMHEL MO £
SAMPLE NO 0
REPORT HO £02
FILE
METHOD
9
Q88£
PKMO
TIME
AREA MK IDHO
CONC
NAME
1
£
3
2.506
2.597
2.792
24500
1319 V
486 V
1
£
94.8925 METHANE
5.1075 ETHANE
TOTAL
26225
100
-------
57/65/19
I C . <"| ET .
I J • j J •
LASCO BAG SAMPLES
(#-5-3)
:.583
CR581 CHRQMATOPAC
CHANNEL HO £
SAMPLE HO 8
REPORT HO £86
PKNO
TIME
TOTAL
AREA UK IDNO
FILE
METHOD
CONC
y
OG02
107£24
NAME
1
£
3
£.503
£.595
£.797
18E146
4898 V
979
1
£
96. 1426
3.8574
188
4
K.
-------
:HROMATOGRAM IQI MEMORIZED
37/95/19 16:£4:0£
LASCQ BAG SAMPLES
65*3
F-- £.798
CR5B1 CHROMATOPAC
CHANNEL NO £
SAMPLE NO 8
REPORT NO £19
2.594
I
g
1
PKNO
TIME
AREA MK IDHO
FILE
METHOD
COHC
NAME
1
£
3
2.504
£.596
£.798
192868
4119 V
967
1
£
96.1592
3.8498
TOTAL 197954
CHROpJOGRAM 101 MEMORIZED
% (37/05/19 16:31:56
WARNING HO PEAK
CHROMATOGRAM 191 MEMORIZED
WARNING HO PEAK
1GO
LASCO BAG SAMPLES
-------
CHRQNAT
CR5B1
CHANNEL
SAMPLE
REPORT
PKNO
1
£
2
4
5
OGRAtl 1G1 MEMORIZED
?7/Q5/l9 16:37:48 LASCO BAG SAMPLES
-
>
h 2.8 1 5 A "
CHROHATOPAC
NO £ FILE 9
HO 8 METHOD 8082
HO 211
1
1
2
£
2
TIME AREA MK IDHO CONC NAME
.484 663
.456 1374 V
.522 13822 1 94.883 METHANE
.613 745 V £ 5.117 ETHANE
.815 126
to
CS&
2.522
TOTAL
16729
100
-------
97/05/19
17:49:£7
LASCO BAG SAMPLES
.497
CR5B1 CHROnftTOPAC
CHANNEL NO £
SAMPLE HO 0
REPORT HO £16
FILE
METHOD
9
GGD£
PKNO
1
£
3
TIME
£.497
£.588
£.79
AREA MK IDHO
84288
3454 V
16654 V
COHC
96.0639
3.9361
NAME
METHANE
ETHANE
-------
37/G5/19
18:88:34
LASCO BAG SAMPLES
o 40
2:732
CR501 CHROttATOPAC
CHANNEL HO £
SAMPLE MO 0
REPORT HO £18
PKNO
TIME
TOTAL
AREA MK IBNO
FILE
METHOD
COMC
9
000£
97146
HAHE
£.49
2.581
2.732
78405
3230
15511
V
'./
1
£
96.8435
3.. 9565
100
-------
TOTAL
97/05/19
1264436
18:32
19
18Q
LA8CO BAG
SAMPLES
CR581 CHROHATOPAC
CHAHHEL NO £
SAMPLE WO 8
REPORT NO £20
PKHO
1
Z
TItlE
2.496
£.586
2.789
TOTAL
AREA HK I DUO
FILE ;
HETHOU
COHC
9
0B8S
HAI1E
1831.1
10Q9
1556S
34883
94.7756 METHAHE
5.£244 ETHANE
189
/I',
-------
TOTAL
37/95/19
4921430
18:52:39
IDG
LASCO BAG SAMPLES
o
OJ
.788
2.494
CR5Q1 'CHROMATOPAC
CHANNEL NO £
SAMPLE HO 8
REPORT HO ££2
PKMO
TIME
3
2.494
2.585
2.733
16205
895 V
11603 V
AREA UK I DUO
TILE
METHOD
COMC
q
0002
NAME
TOTAL .28703
CHROMATOGRAM 101 MEMORIZED
97/05/19 19:91:49
94.7689 METHANE
5.2311 ETHANE
100
LASCO BAG SAMPLES
CR501 CHROMATOPAC
CHANNEL HO £
SAMPLE MO 9
REPORT HO
£23
PKNO
1
2
3
TIME
2.498
2.587
2.788
AREA MK IDNO
FILE
HETHOD
COMC
9
9002
NAME
16410
993 V
13096
TOTAL 36409
CHROMATOGRAM 101 MEMORIZED
1
2
94.7331 METHANE
5.2169 ETHANE
100
-------
CHROMATOGRAM 101
57/95/19
MEMORIZED
19:55:38
LASCO BAG 'SAMPLES
£.491
CR501 CHROMATOPAC
CHANNEL HO £
SAMPLE HO 8
REPORT HO £30
FILE
METHOD
9
8BG£
o
CJl
•3
F'KMO
IME
AREA MK IDHO
CONC
NAME
1 2.491
£ £.533
3 £.755.
TOTAL
CHROMATOGRAM 101
57/95/19
186894
4370 V
1016 V
11££88
MEMORIZED
£0:08: IB
1 96.87
£ 3.9S
•
100
LASCO BAG
£1 METHANE
78 ETHANE
SAMPLES
IO
NO
u>
6
CO
VJ
6
KJ
£.78
2.492
CR5D1 CHROMATOPAC
CHANNEL HO £
SAMPLE NO
REPORT NO
PKNO
0
£31
TIME
AREA MK IDHO
FILE
METHOD
COHC
9
000£
MAI1E
1
£
3
2.492
£.584
£.785
104139
4£61
985
V
V
1
£
TOTAL
109385
96.0693 METHANE
3.9307 ETHANE
108
-------
CHROMATOGRAM 101
?7/05/19
MEMORIZED
£8:12:34
•JOC
LASCO BAG SAMPLES
1.491
CR5G1 CHROMATOPAC
CHANNEL HO £
SAMPLE MO 0
REPORT NO £3£
PKHO
71 HE
AREA
MK
IDNO
FILE
METHOD
COMC
9
8002
NAME
1, 2.491
2 2.582
3 2.784
TOTAL
CHROMATOGRAM 101
97/05/19
25129
1362 V
£76 V
2 6 7 6 7
MEMORIZED
20:17:12
1 94.8572
2 5.1428
100
METHANE
ETHANE
LASCO BAG SAMPLES
2.491
CR501 CHROHATOPAC
CHAHMEL MO 2
'ILE
SAMPLE
REPORT
PKNQ
1
£
3
MO 0
NO 233
TIME
2.491
2.58£
£.734
AREA
23202
1251
26£
MK
V
V
r
I DUO
1
E.
IETHOD G
CONC
94.3847
5.1153
1002
NAME
METHANE
ETHAME
TOTAL
24715
109
-------
CHROMATOGRAM 191 MEMORIZ
37/95/19 £9: £'6: 4
| £.784
CR591 CHROMATOPAC
CHAMMEL HO £
SAMPLE HO 9
REPORT HO £34
PKHO TIME AREA
1 . £.491 192699
£ £.583 4163
3 £.784 969
TOTAL 167739
CHROHATOGRAM 101 MEMORIZ
37/85/19 £0:34:£
[ £.786
CR5G1 :HROMATOPAC
CHAMMEL HO £
SAMPLE HO 8
REPORT HO £35
PKHO TIME AREA
1 £.493 1Q51S9
£ £.585 4£49
3 £.786 981
ED "" * *
1 LASCO BAG SAMPLES C6$J
,
FILE 9
METHOD 9992
NK I DUO COMC MAME
1 96. 1014 METHANE
£ 3.8986 ETHAME
'„'
180
ED - >'; 9^
6 LASCO BAG 'SAMPLES C6&
i
FILE 9
METHOD 9992
MK IDHQ COMC NAME
1 96. 1176 METHflME
V £ 3.8824 ETHAME
$
b
Ml
pl
I
\
\
1
TOTAL
110418
1Q9
-------
CHROHATOGRAtt 101
•J7/85/19
MEMORIZED
£6:39:16
LASCO BAG SAMPLES
2.493
o
ci
CR581 CHROMATOPAC
CHANNEL HO £
SAMPLE MO 8
REPORT. NO £36
PKMQ
1
cl
•-I
•J
• TIME
£.493
£.584
£.786
AREA
24219
1280
£9G
FILE
METHOD
CONC
9
8002
NAME
TOTAL
£5789
94.9786 METHANE
5.GE14 ETHANE
100
N>
ro
CO
6
8
CJ
•VI
6
ro
ctf
-------
CHROMATOGRAM 191
57/05/19
MEMORIZED
£8:43:50
£.787
LASCO EAG SAMPLES
<;<,&
2.494
CR501 CHROMATOPAC
CHANNEL MO £
SAMPLE MO 8
REPORT MO
37
FILE
METHOD
008S
PKNO
1
£
3
TIME
£.494
£.585
£.737
TOTAL
d. tl • 4 b • o-£r^
AREA UK
£1997
1149 V
£49 V
£3395
<•' 9 j / 1 5
IDNO CONC
1 95.0377
£ 4.96££
100
•* LASCO TUEES
NAME
METHANE
ETHANE
CHROMATOGRAM 1
WARNING NO PEAK
97/05/ly9
MEMORIZED
£0:50:58
LASCO EAG SAMPLES
2.491
CR501 CHROtlATOPAC
CHAMMEL MO £
SAHPLE MO 8
REPORT MO 238
FILE
METHOD
£
PKHO
1
2
3
TIME
2.491
2. 532
2.784
AREA
20500
1080
225
MK
V
IDMO
1
2
CONC
94.9931
5.0069
TOTAL
21805
MAME
100
-------
,iiKlinATQGRAM 101
*7/95/£2
MEMORIZED
17: 00: £9
LASCO BAG SAMPLES
2.499
CR501 CHROMATOPAC
CHANNEL NO £
SAMPLE MO 0
REPORT NO 37
PKMO
TIME
AREA MK IDNO
FILE
METHOD
COHC
9
08B£
NAME
£656
METHAME
E7HAHE
TOTAL
1S5S9
-------
TOTAL
£41728
16:03:49
F
10B
LASCO BAG
SAMPLES
2.496
CR501 CHROMATOPAC
CHfiMMEL HO £
SAHPLE NO 9
REPORT NO 34
FILE
I1ETHQD
q
08B2
PKMO
TIME
AREA f1K I UNO
COMC
MAME
£.496
£.585
£.79
16968
1346
475
£
9£.65G8 METHANE
7.349£ ETHAME
-------
TOTAL
97/85/22
927835
15:28:58
'£.79
108
LASCO BAG SAMPLES
2.497
CR581 CHROI1ATOPAC
CHANNEL NO 2
SAMPLE MO 8
REPORT NO 30
PKNO
r
TIME
2.497
2.5S8
AREA UK IDM0
91681 1
3571 V £
88'8 V
FILE
METHOD
COMC
9
0892
NAME
96.2508 METHANE
3.7492 ETHANE
-------
TOTAL
97/05/2£
939286
14:59:24
109
LASCO BAG
AMPLES
2.796
2.501
CR581 CHROMATQPAC
CHANNEL NO £
SAMPLE NO 8
REPORT MO 28
FILE
METHOD
9
9082
PKHO
2
3
TIME
£.501
£.594
£.796
TOTAL
AREA MK I DM0
99911 1
3601 V £
794 V
953G6
CO NO-
96. 1895 METHANE
,3, SI 05 ETHANE
1 Of)
i
-------
TOTAL
CHROMATOGRAI1 101
187584
MEMORIZED
11:48:11
168
LASCO BAG SAMPLES
2.489
CR5Q1 CHROI1ATOPAC
CHANNEL HO £
SAMPLE NO 0
REPORT NO 17
PKNO
TIHE
AREA MK IDNCi
FILE
METHOD
COHC
NAME
1 2.489
£ £.578
3 £.781
TOTAL
HROMATOGRAM 1Q1
37/65/££
19737
1406 V
681 V
£18£5
MEMORIZED
ll:5£:41
1 93.3484
£ 6.6516
106
METHANE
ETHANE
LASCO BAG SAMPLES
£.751'''
2.489
CR5Q1 CHROMATOPAC
CHANNEL NO £
FILE
SAMPLE
REPORT
-(NO
1
£
3
NO 0
NO 18
TIME
£.489
£.578
£.781
METHOD 000£
AREA MIC IDNO
£0£39 1
14£9 V £
668 V
CONC NAME
93.4068 METHANE
6.593E ETHANE
TOTAL
££336
100
-------
CHRQMATOGRAH 101
37/85/22
MEMORIZED
2.78
LASCO BAG SAMPLES
£.438
CR5B1 CHROtlATQPAC
CHAMMEL NO 2
SAMPLE NO 0
NO
REPORT
15
FILE
METHOD
9
000£
PKNO
;1
'•2
1'
T
c .
-I
U i
2.
I ME
43
c 7
73
3
9
AREA MK IDNO
101
0
71
97
2 1
1 V £
CONC
96. £4
3, 75
NAME
£2
{'
8
METHANE
ET
HANE
950 V • M,
TOTAL 106633
CHROMATOGRAM 101 MEMORIZED
37/85/22 11:43:59
2.783
CJ
6
N)
100
LASCO BAG SAMPLES
2.489
CR5B1 CHROMATOPAC
CHANNEL NO 2
SAMPLE NO 8
REPORT NO 16
PKNO
TIME
AREA MK IDNO
FILE
METHOD
CONC
9
0002
NAME
1
£
3
2.
2.
2.
489
581
733
1
82614
4811
959
V
V
1
£
96.
<-,
O •
238
761
1
9
METHANE
ETHANE
-------
;:-iKonflTOGRftn IBI MEMORIZED
97/85/22
11:15: 10
LASCQ BAG SAMPLES
2.436
CR581 CHROMATOPAC
CHftHMEL 110 2
SAMPLE HO 8
REPORT HO 13
FILE
METHOD
PKHO
TIME
AREA hK IDHO
CONC
NAME
2
2.486
£.578
TOTAL
CHROMATOGRAM 101
97/65/22
16365
6070
£24
MEMORIZED
ll:£3:£3
72.9448 METHANE
27.0552 ETHANE
100
LASCO BAG SAMPLES
2.485
CR5Q1 CHROMATOPAC
CHANMEL MO £
SAMPLE HO 0
REPORT HO 14
FILE
METHOD
9
0902
PKHO
1
£
TIME
£.485
£.5;
•577
AREA MK IDHO
15413
5751
1
£
COMC
HA ME
72.8251 METHANE
£7.1749 ETHAME
TOTAL
£1164
100
-------
;HROMATQGRAM 101
"•> ? / O 5 / £ £
MEMORIZED
10:49:11
LftSCO BAG SAMPLES
2.433
CR5G1 CHROMATOPAC
CHANNEL HO 2
SAMPLE HO 8
REPORT HO 11
FILE
METHOD
9
8802
?KNO
TIME
AREA MK I UNO
COHC
HAtlE
£.483
• 2.574
55987
33Q1 V
TOTAL 55288
CHROMATOGRAM 101 MEMORIZED
?7/85/22
18:55:33
94.4324 METHANE
5.5676 ETHANE
108
LASCO BAG SAMPLES
n t
!.433
CR501 CHROMATOPAC
CHAHHEL HO 2
SAMPLE HO 8
FILE
METHOD
9
000E
REPORT HO 1£
PKMO TIME
£.433
£.575
AREA MK IDM0
56£99
3313
1
£
COMC
NAME
94.443£ METHAME
5.5568 ETHANE
K>
ro
TOTAL
5961£
100
-------
'7/05/22 10:31:50 LASCO BAG SAMPLES
• £.775 I"J<0
•?-*- 1
CR501 CHROMATOPAC
CHANNEL NO £ . FILE 9
SAMPLE NO 0 METHOD 0002
REPORT HO 9
PKNO
1
C
3
TIME AREA MK I UNO CONC NAME
£.483 183959 1 96.1028 METHANE
£.575 4216 '
CHROMATOPAC
. NO 2 FILE 9
NO 9 METHOD 0002
NO 10
TIME AREA MK IDNO CONC NAME
2.484 45549 1 96.0425 METHANE
£.576 1877 V £ 3.9575 ETHANE
2.777 597 V
K3
CJ
W
CJ
6
8
U>
g
\lQUWl
€
u
r
r
TOTAL
48024
109
-------
JHRQHATOGRAtl 131
97/05/22
MEMORIZED
lBs£0:i£
. % m J* I >.'
., f / b
LASCO BAG SAMPLES
I
2.434
CR5B1 CHRQMATQPAC
CHANNEL HO £
SAMPLE HO S
REPORT NO 7
PKNO
TIME
AREA MK IDNO
FILE
METHOD
CONC
9
D0B2
NAME
1
2
3
CKROHAT
2.434
' £.573
£.776
TOTAL
OGRAM 181
18811
1478 V
674 V
'"i £"| Q j* ^t
d w 7 O Of
MEMORIZED
iQ: 25: 16
1 92
£ 7
188
•••! -LASCO E
.7172 METHANE
.£828 ETHANE
AG SAMPLES
2.484
CR581 CHROttATOPAC
CHANNEL NO £
SAMPLE NO 8
REPORT HO 8
FILE
METHOD
9
0DB2
PKNO
TIME
AREA MK IDHO
COHC
NAME
1
£
V
IOMA
2.484
£.573
2.776
TOTAL
TOGRAM 181
18879
1477 V
672 V
21028
MEMORIZED
92.743 METHANE
7.£57 ETHANE
188
-------
TOTAL
oROMATOGRAM 1Q1
£17859
MEMORIZED
10:86:89
1QB
LASCO BAG SAMPLES
2.48£
CR501 CHROMATOPAC
CHANNEL HO £
SAMPLE HO 8
REPORT HO 5
FILE
METHOD
Q
0002
PKMO
1
c
TIME
£.482
£.573
AREA MK IDNO
24473
4479
TOTAL £895£
CHROMATOGRAM 101 MEMORIZED
37/85/22 10:12:34
CQNC
NAME
84.5306 METHANE
15.4694 ETHANE
1QG
LASCO BAG SAMPLES
2.432
CR561 CHROMATOPAC
CHANNEL HO £
SAMPLE NO 0
REPORT HO 6
FILE
METHOD
9
9882
PKNO
1
£
TIME
2.48£
2.572
TOTAL
AREA MK IDMO
£3572
4290
E786£
1
,£
10
10
COMC
HAME
84.60£9 METHANE
15.3971 ETHANE
100
to
to
-------
•-ROMATOGRAM 181
i7/85/c'£:
MEMORIZED
Q9:45:4 6
LASCO BAG SAMPLES
CR501 CHROMATOPAC
CHAM MEL HO £
SAMPLE NO 0
REPORT HO 3
FILE
METHOD
GOGS
PKMO
1
£
TIME
£.479
£.566
AREA MK I UNO
1
156054
53094
TOTAL £99148
CHROMATOGRAM 101 MEMORIZED
37/Q5/S2 09.: 53:38
CO.NC
HA ME
74.6142 METHANE
£5.3858 ETHANE
100
LASCO BAG SAMPLES
CR501 CHROMATOPAC
CHANNEL HO £•
SAMPLE NO 0
REPORT NO 4
PKMO TIME AREA MK IDNO
1 2.481 162487 1
£ £.573 55363 V £
FILE
METHOD
CONC
9
000S
NAME
74.5868 METHANE
£5.4132 ETHAHE
to
-------
CHROMATGGRAM 1 MEMORIZED
JARHING NO PEAK
JHROMATOGRAM 101 MEMORIZED
CR561
CHANNEL
SAMPLE
REPORT
'7/65/22 69:26:35
CHROMATOPAC
NO 2
•iO 6
NO 1
PKNO TIME AREA UK
1
CHROMAT
CR561
CHANNEL
SAMPLE
REPORT
2.475 15477
TOTAL 15477
OGRAM 161 MEMORIZED
?7/65/22 09: £9: 06
:HROMATOPAC
. NO £
NO e
NO £
PKNO TIME AREA NK
1
2.48 15535
TOTAL 15535
LASCO.BAG SAMPLES
FILE 9
METHOD OOOS
IDNO CONC NAME
1 166 METHANE
18Q
LASCO BAG SAMPLES
FILE 9
METHOD 6662
I UNO CONC NAME
1 100 METHANE
166
tf>
2.475
2.43
-------
£1:40:38
LASCO BAG SAMPLES
0-10-
•-' ^CiV
£.78
CR501 CHROMATOPAC
CHANNEL NO 2
SAMPLE NO 0
REPORT HO 48
PKNO
1
£
TIME
£.496
£.585
£.738
TOTAL
AREA MK IDNO
1398£
1£73 V
133££
33577
FILE
METHOD
CONC
9
000S
NAME
93.7146 METHANE
6.£854 ETHANE
109
I
-------
£1:36:34
LH&tU DMU an in 1.1.
:.79l
2.497
CR581 CHROtlftTOPAC
CHflMHEL NO £
SAMPLE MO 8
REPORT NO 47
:'KMO
TIME
AREA MK IDNO
FILE 9
METHOD B(
COHC
' TOTAL 33767
C'HROHATOGRAfl 101 MEMORIZED
NAME
1
2
3
2,497
£.587
£.791
19083
1282
13492
V
1
£
93.7942
6. £958
100
-------
37/85/££
LASCO BAG SAMPLES
-9-]
£.499
CR581 CHROI1ATOPAC
CHANNEL NO £
SAMPLE HO 0
REPORT NO 42
'KNO
1
TIHE
£.499
£.589
£.793
TOTAL
;HRO!1ATOGRAI1 191
AREA UK I DUO
11779
777
£13
FILE
METHOD
CONC
9
9682
NAME
1£769
MEMORIZED
2
93.8985 METHANE
6.1915 ETHANE.
196
-------
CR5Q1
CHANNEL
SAMPLE
REPORT
-'KNO
1
2
3
^7/95/22 cC
C"~ •:• "70*4* *
r c « (" o o .
CHROttftTOPAC
HO £
HO 8 '
HO 41
TIME
2,493
£.588 •
•. 2.783
TOTAL
CHROMftTQGRftH 101 11
4:47:52
AREA UK
1E469
824 V
24S V
13532
EHORIZED
LASCO BAG SAMPLES /
FILE 9
METHOD 8082
IDHO CONC NAME
1 93.8844 METHANE
2 6.1956 ETHANE
108
2.498
-------
£6:38133
F £. 792""'
LASCO BAG SAMPLES
£.438
CR5B1 CHRQMATOPAC
CHANNEL NO £
SAMPLE HO 9
SEPORT MO 4G
TIME
£.493
£.59
AREA MK IDHO
3£85Q i
1455 V £
£84 V
TILE
HETHOD
COHC
988£
NAME
95.7532 METHANE
4.£416 ETHANE
to
I
X4
TOTAL
;HROHATOGRAH IGI
34589
MEMORIZED
190
-------
CR591
CHANNEL
SAMPLE
^7/95/22 20:32:14 LASCO BAG SAMPLES
p 2.794U*J'U
CHROHATOPAC
NO 2 FILE ' ' 9
NO 0 METHOD 0002
REPORT NO 39
PKNO
1
£
o
TOTAL 39194
CHROHATOGRAM 101 MEMORIZED
TIME
£.499
£.592
£.794
AREA
37234
1S4?
313
!1K
v
\i
IDNO
1
C
CONC
NAME
£.499
95.764 METHANE
4.£359 ETHANE
1Q8
-------
T
u .
£ .
c. •
I ME V.
499
5 9 £
794
, ..AREA MK
48419
1 7 9 0 V
347 V
IBND
1
£
CONC
95.
4.
73S£
£418
NAME
METHAME
ETHANE
TOTAL 4£556
::-iROMATOGRAM 1G1 HEMORIZED
100
I
;,HROMATOGRAH 101 MEMORIZED
C:\56i CHROHATOPAC
ChAHHEL HO £
3AMPIE MO 3
*:PQ;RvT MO 38
LASCO SAG SAMPLES
EIH 0 D
-9-1
2.499
-------
APPENDIX C
CALCULATIONS
-------
Example Calculations for Pollutant Emissions
1 . Volume of dry gas sampled corrected to standard conditions, ft3. Note: Vm
must be corrected for leakage if any leakage rates exceed La.
Vmstd = 17 .647 x Vm x Y 13 ' 6
Tm
2. Volume of water vapor at standard conditions, ft3.
Vwstd = 0.04707 x Vic
3. Moisture content in stack gas, dimensionless.
Vwstd
Bws =
Vwscd + Vmstd
4. Dry molecular weight of stack gas, Ib/lb-mole.
Md = 0.44(%C02) * 0.32(%O2) + 0.28(%tf2 * %CO)
5. Molecular weight of stack gas, Ib/lb-mole.
Ma = Afd(l - Bws) + IBBws
6. Stack velocity at stack conditions, f/s.
Vs = (85.49) (Cp) (avgJFP) J Ts
(PS)(MS)
7. Stack gas volumetric flow rate at stack conditions, cfm.
Qs = 60 x Vs x As
8. Dry stack gas volumetric flow rate at standard conditions, cfm.
Qsstd = (17.647) (Qs) [-P1 (1-Bws)
-------
9. Concentration in gr/dscf.
Mn
Cs = (0.01543)
10. Pollutant mass emission rate, Ib/h.
Vmstd
pmr, Ib/hi = f Cs \ x Qsstd x 60
\7000/
11. Pollutant mass emission rate, Ib/mmbtu
pmr, Ib/rmbtu- (f
(mmbtu/hr)
12. F-factor(Fd)
106 (3. 64 *%#) + (!. 53 x%C) + (0.57x%S) + (0 .14x%tf) - (0 . 46x%O2)
13. F-factor, pollutant mass emission rate, Ib/mmbtu
- Ib/dscf x F x 20.9
, = (20.9 - % 02)
14. Heat input, mmbtu/hr fuel
_ <7VC (btu/lb) » Feed Rate (Ib/hx)
106
15. Heat Input, mmbtu/hr, F-f actor.
= gggt'd X ((20.9 - %02) * 20.9) X60
-------
Nomenclature and Dimensions
An = Cross-sectional area of sampling nozzle, sq. ft.
As = Cross-sectional area of stack, sq.ft.
Bws = Proportion by volume of water vapor in the gas stream, dimensionless
Cp = Pltot tube coefficient, dimensionless
Cs = Concentration of pollutant matter in stack gas - dry basis, grains per
standard cubic foot (gr/dscf)
% CO = Percent of carbon monoxide by volume, dry basis
%CO2 = Percent of carbon dioxide by volume, dry basis
AH = Average pressure drop across the sampling meter flow orifice, inches
of water (in. H2O)
GCV = Gross calorific value, btu/lb
= Percent of Isokinetic sampling
La = Maximum acceptable leakage rate for either a pretest leak check or for
a leak check following a component change; equal to 0.020 cubic foot
per minute or 4% of the average sampling rate, whichever is less
Md = Dry molecular weight, Ib/lb-mole
Mn = Total amount of pollutant matter collected, miiligrams (mg)
Ms = Molecular weight of stack gas (wet basis), Ib/lb-mole
%N2 = Percent of nitrogen by volume, dry basis
%O2 = Percent of oxygen by volume, dry basis
AP = Velocity head of stack gas, Inches of water (In. H2O)
Pbar = Barometric pressure, inches of mercury (In.Hg)
Ps _= Absolute stack gas pressure, Inches of mercury (In.Hg)
Pstd = Gas pressure at standard conditions, inches of mercury (29.92 In.Hg)
-------
pmr = Pollutant matter emission rate, pounds per hour (Ib/h)
Qs = Volumetric flow rate - wet basis at stack conditions, actual cubic feet
per minute (acrm)
Qsstd = Volumetric flow rate - dry basis at standard conditions, dry standard
cubic feet per minute (dscfm)
Tm = Average temperature of dry gas meter, °R
Ts = Average temperature of stack gas, °R
Tstd = Temperature at standard conditions, (528°R)
Vic = Total volume of liquid collected in impingers and silica gel, ml
Vm = Volume of dry gas sampled at meter conditions, cu. ft.
Vmstd = Volume of dry gas sampled at standard conditions, cu. ft.
Vs = Average stack gas velocity at stack conditions, ft/s
Vwstd = Volume of water vapor at standard conditions, set
Y = Dry gas meter calibration factor, dimensionless
0 = Total sampling time, minutes
NOTE: Standard condition = 68°F and 29.92 In.Hg
-------
EXAMPLE CALCULATIONS FOR POLLUTANT EMISSIONS
GASEOUS POLLUTANTS MEASURED BY
CONTINUOUS EMISSIONS MONITORS (CEMs)
1) Concentration, part per million, dry basis:
. t • /, , ,
ppm, dry = ppm, wet basis * (I- ——)
1UU
2) Pollutant Mass Emission -.Rate, pound per hour.
PAffl, Iblhr = ppm* dry X ComP°und Molecular Weight x ^^ x 6Q
(385.3 x 10 6)
Molecular Weights of Target Compounds
TOO = Total Gaseous Organics 44.09
SO2 = Sulfur Dioxide 64.05
NO2 = Nitrogen Oxides 46.00
CO = Carbon Monoxide 28.01
BWS = Proportion by Volume of Water Vapor in the Gas Stream
PMR = Pollutant Mass Emission Rate, Pound Per Hour
-------
EXAMPLE CALCULATIONS FOR POLLUTANT EMISSIONS
NIOSH/OSHA METHODS AND EPA METHOD 18
1) Sample Volume, Standard Liters (Evacuated Tank)
17.647 x T.V., liters x ( &[- ^ }
T.V, = Calibrated total tank volume, liters
Pf = Final tank pressure, in. Hg (Pbar, "Hg-Final tank vacuum. "Hg)
Pi = Initial tank pressure, in. Hg (Pbar. "Hg-Initial tank vacuum. "Hg)
Tf = Final tank temperature, °R
Ti = Initial tank temperature, °R
2) Sample Volume, Standard Liters (VOST Meter)
(Tm, Q
Vm = Volume of gas metered, liters
Pbar, "Hg = Barometric pressure, inches of mercury
Tm, °R = Average meter temperature, °Rankin
Y = Gamma factor of Yost Meter
3) Concentration, micrograms per li
» Total ugfsample * Vmstd, liters
-------
EXAMPLE CALCULATIONS FOR POLLUTANT EMISSIONS
NIOSH/OSHA METHODS AND EPA METHOD 18
4) Concentration, part per million, wet basis
ugfliter x 24.04 literfmole
ppm, wet = —
MW, analyte
5) Concentration, part per million (ppm), dry basis
ppm, dry = ppm, \ver/(l-//2O%/100)
6) Mass Emission Rate, pound per hour
r = ppm, dry X MW, analyte
(385.3 x 106)
mg = Micrograms, total
MW = Molecular weight of target analyte
ppm = Part per million
Qsstd, dscfm = Volumetric stack gas flow rate, dry standard cubic feet per
minute
MR, Ib/hr = Mass emission rate, pound per hour
Molar volume = 385.3 fl?/lb mole
PPM by Volume = ft3 . volume ratio
-------
^PACIFIC ENVIRONMENTAL SERVICES, INC.
USEPA - Lasco Panel Products
Florence, KY
uaie
8ll5
uy
ine""ue
Sample Calculations
Main Exhausr - Condition 1. Run
1) Concentration, ppm, dry basis:
1-
BWS,%
100
2965.4
1-
100
2) Concentration as Styrene, ppmdr
.*™* = PPm,ir, x response factor^
ivn-ne
xlynm = 3013.6 x 0.4263 = \2M.1 ppm. y
3) Styrene Mass Emission Rate (MR), Ib/hr
, x MolecularWeiShtcompountl
385 xlO6
1284.7x104.15
x flowratelbcfm x 60
7
xlryene
385 xlO6
x 3378 x 60 = 70.44 Ib/hr, as styrene
Natural Draft Oenin NDOt Austment Calculations1 - NDO, Condition 1. Run 1
1) Flow Factor, %
flowfactor =
flowfactor =
NDO
Afjm
(NDOA + NDOB + NDOC + NDOD\
7334
(7334 + 138 + 665 + 531)
'CJm
= 0.84 = 8.4%
2) Adjusted Concentration (AC), ppm
1 Note that the room exhaust, auxiliary exhaust and Natural Draft Opening (NDO) calculations are the
same as the above examples for main exhaust
2 Note that the NDO adjustment calculations apply to NDOA> NDOB> NDOC and NDOD.
WASHINGTON, DC • RESEARCH TRIANGLE PARK, NC • LOS ANGELES, CA • CINCINNATI, OH
-------
OPACIFIC ENVIRONMENTAL SERVICES, INC.
ffil*Dy
U3l£ j.
^uecKca oy
4532. U^u . 7 i.
^
cilcm
USEPA - Lasco Panel Products
L0tailon Florence, KY
Sample Calculations
inialrunx
^ Concentration
run I
ppm
run
x Jlowfactor
total
(6.1 + 5.0 + 6.9)
= -^ ^x.84 = S.Qppm
3) Total NDO Adjusted Concentration, ppmwet
ppm
NDO,olal = 5.0 + 0.1 + 0.7 + 0.6 = 6.5ppm,,.,
'•*..
*
Concentration adjustment and conversion calculations
1) Concentration as propane, ppmwet
= Total ppmwet-NDOadj)ppm
= 2553.6-11.0 = 2542.6 ppm
2) Concentration conversion, propane to carbon, ppm
Cc = Cp * Kp Kp=3 (40 CFR Pt. 60, App A, Meth. 25A)
Cc = 43.5* 3 = 130.5 ppm
3) Concentration conversion, methane to carbon, ppm
Cc = Cm * K,,, ^=1 (40 CFR Pt. 60, App A, Meth. 25A)
Cc = 83.1* 1=83.1 ppm
4) Concentration conversion, ethane to carbon, ppm
Cc = Ce * K, K,=2 (40 CFR Pt. 60, App A, Meth. 25A)
Cc = 3.1 *2 = 6.2ppm
WASHINGTON, DC • RESEARCH TRIANGLE PARK, NC • LOS ANGELES, CA • CINCINNATI, OH
-------
OPACIFIC ENVIRONMENTAL SERVICES, INC.
WJCtyjT 'U QY U3 6
LnecKeo oy
,-ruJcc^0. 4532.020
t'UEC Ol
" 3 3
ciiuu
USEPA - Lasco Panel Products
LUUU'°" Florence, KY
3nc"""e Sample Calculations
Total Overall Enclosure Exhaust. Ib/hr as styrene - Condition 1 r Run 1
= ( MR^^.^ + MR,,,,,,,,^^ + MR,^,^^^, + MRNDOloUi) Ib/hr as styrene
= 70.44 + 13.11 + 0 - 0.38 = 83.17 Ib/hr as styrene
WASHINGTON, DC • RESEARCH TRIANGLE PARK, NC • LOS ANGELES. CA • CINCINNATI. OH
-------
PACIFIC ENVIRONMENTAL SERVICES, INC.
Project No.
5 ^ 05
Page
of
Client
Location
/> c
Prepared By
Date
Checked By
Date
Sheet Title
61
•A|
,
/~ ."-
/t
^C
''9
^*
I j
ft
/k 7"
-------
61'
Outside
Natural Draft Opening (NDO) - A
(32" X 120")
Oven Area
82'
NDO-B
(0.5" X 72")
Fresh Air Supply
(14"X26")
NDO-C
Doorway
(Closed)
(36" X 84")
Doorway
(Closed)
(36" X 84")
Doorway
(Closed)
(36" X 84")
Overhead Door
(Closed)
(96" X 120")
Main Exhaust
(17.5")
Overhead Door
(120"X168")
(Closed)
Fresh Air Supply
(14" x 26")
NDO-D
Doorway
(Closed)
(36" X 84")
Auxilary Fan
Outside
(19.75")
Room Exhaust
(24" X 28")
Air Sampling
THC
Styrene
Cumene
Methyl Methacrylate
-------
Lasco-EPA
Sui
Ov
Condition Run
1 1
1 2
1 3
Average
2 1
2 2
2 3
Average
3 1
3 2
3 3
.(4 wage
4 1
4 2
4 3
Average
5 I
5 2
5 3
Average
6 1
6 2
6 3
/I wage
7 1
7 2
7 3
Average
8 1
8 2
8 3
/4wa#«
9 1
10 1
11 1
M25A
propane
ppm
118.7
132.3
128.2
126.4
50.4
71.9
108.0
76. 8
87.9
118.9
106.4
104.4
110.1
113.4
NA
111.8
149.8
164.1
139.8
151.2
156.3
161.4
167.2
161.6
146.3
121.8
109.9
126.0
112.9
131.5
110.8
118.4
67.0
110.9
59.2
M25A
propane
to carbon
ppm
356.1
396.9
384.6
379.2
151.2
215.7
324.0
2 30. 3
263.7
356.7
319.2
313.2
330.3
340.2
NA
335.3
449.4
492.3
419.4
453.7
468.9
484.2
501.6
484.9
438.9
365.4
329.7
378.0
338.7
394.5
332.4
355.2
201.0
332.7
177.6
GC
methane
ppm
282.7
313.3
307.6
301.2
230.8
215.7
263.2
236.6
154.9
276.3
240.9
224.0
258.6
254.0
NA
256. 3
339.4
317.4
274.1
310.3
216.1
282.4
277.9
258.8
304.6
200.9
184.3
229.9
331.8
326.1
291.2
316.4
123.1
190.9
. 162.2
GC
methane
to carbon
ppm
282.7
313.3
307.6
301.2
230.8
215.7
263.2
236.6
154.9
276.3
240.9
224.0
258.6
254.0
NA
256. 3
339.4
317.4
274.1
310.3
216.1
282.4
277.9
258.8
304.6
200.9
184.3
229.9
331.8
326.1
291.2
316.4
123.1
190.9
162.2
GC
ethane
ppm
7.1
7.7
7.7
7.5
5.9
5.7
6.9
6.2
4.2
6.7
5.9
5.6
6.6
6.7
NA
6.7
9.1
8.6
7.2
8.3
5.8
7.6
7.4
6.9
8.1
5.4
4.8
6.1
8.8
8.3
7.5
8.2
3.4
4.9
4.5
GC
ethane
to carbon
ppm
14.2
15.4
15.4
15.0
11.8
11.4
13.8
12.3
8.4
13.4
11.8
11.2
13.2
13.4
NA
13.3
18.2
17.2
14.4
16.6
11.6
15.2
14.8
13.9
16.2
10.8
9.6
12.2
17.6
16.6
15.0
16.4
6.8
9.8
9.0
Total
carbon
ppm
59.2
68.2
61.6
63.0
0.0
0.0
47.0
15.7
100.4.
67.0
66.5
78.0
58.5
72.8
NA
65.7
91.8
157.7
130.9
126.8
241.2
186.6
208.9
212.2
118.1
153.7
135.8
135.9
0.0
51.8
26.2
26.0
71.1
132.0
6.4
Total
propane
ppm
19.7
22.7
20.5
21.0
0.0
0.0
15.7
5.2
33.5
22.3
22.2
26.0
19.5
24.3
NA
21.9
30.6
52.6
43.6
42.3
80.4
62.2
69.6
70.7
39.4
51.2
45.3
45.3
0.0
17.3
8.7
8.7
23.7
44.0
2.1
H2O
%
.8
.8
.8
1.8
.3
.2
.1
1.2
.1
.1
.1
.1
.2
.2
NA
1.2
2.8
2.5
2.2
25
2.2
2.2
2.2
22
" .2
.6
.9
1.6
.7
.7
.7
1.7
4.5
0.2
0.5
Total
propane
dry
ppm
20.1
23.2
20.9
21.4
0.0
0.0
15.8
5.3
33.8
22.6
22.4
26. 3
19.7
24.6
NA
22.1
31.5
53.9
44.6
43.4
82.2
63.6
71.2
72.3
39.8
52.1
46.1
46.0
0.0
17.6
8.9
8.8
24.8
44.1
2.1
Response
factor
to
styrene
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
NA
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
Total
styrene
ppm
8.6
9.9
8.9
9.1
0.0
0.0
6.8
2.3
14.4
9.6
9.6
11.2
8.4
10.5
NA
9.4
13.4
23.0
19.0
18.5
35.0
27.1
30.4
30.8
17.0
22.2
19.7
19.6
0.0
7.5
3.8
3.8
10.6
18.8
0.9
M18
styrene
ppm
0.3
0.8
12.5
NA
1.4
1.5
0.2
0.2
1.0
Volumrlrk
flow rate
dscfm
1907.0
1924.0
1927.0
1919.3
1905.0
1870.0
1964.0
1913.0
1855.0
1886.0
1894.0
1878.3
1890.0
1917.0
NA
1903.5
1821.0
1934.0
1958.0
1904.3
1948.0
1942.0
1923.0
1937. 7
1905.0
1898.0
1905.0
7902. 7
1926.0
1927.0
1929.0
1927.3
1839.0
1909.0
1979.0
Mass
Rate
Ib/hr
0.27
0.31
0.28
0.28
0.00
0.00
0.22
0.07
0.43
0.29
0.29
0.34
0.26
0.33
NA
0.29
0.40
0.72
0.60
0.57
1.11
0.85
0.95
0.97
0.53
0.68
0.61
0.61
0.00
0.23
0.12
0.12
0.32
0.58
0.03
CONVSHT.XLS
-------
Lasco-EPA
Conversion Summary Sheet
Oven 9
1
Condition Run
11 2
11 3
Average
12 1
12 3
12 4
Average
13 1
13 2
13 3
Average
M25A
propane
ppm
67.8
71.5
66.2
103.5
130.3
112.9
7/5.6
124.6
130.8
121.8
125.7
M25A
propane
to carbon
ppm
203.4
214.5
198.5
310.S
390.9
338.7
346.7
373.8
392.4
365.4
377.2
GC
methane
ppm
151.1
168.4
160.6
207.4
280.3
256.8
248.2
267.8
291.3
235.5
264.9
GC
methane
to carbon
ppm
151.1
168.4
160.6
207.4
280.3
2S6.8
248.2
267.8
291.3
235.5
264.9
GC
ethane
ppm
4.2
4.5
4.4
6.1
8.4
7.8
7.4
8.2
8.8
7.1
8.0
GC
ethane
to carbon
ppm
8.4
9.0
8.8
12.2
16.8
15.6
74.9
16.4
17.6
14.2
16.1
Total
carbon
ppm
43.9
37.1
29.7
90.9
93.8
66.3
83.7
89.6
83.5
115.7
96. 3
Total
propane
ppm
14.6
12.4
9.7
30.3
31.3
22.1
27.9
29,9 -
278,
38.6"
32.7
mo
":•%'
0.5
0.5
0.5
3.0
3.0
3^0
3.0
1.0
1.6
1.0
7.2
Total
propane
dry
ppm
14.7
12.4
9.8
31.2
32.2
22.8
28.8
30.2
28.3
39.0
32.5
Response
factor
to
styrene
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
Total
styrene
ppm
6.3
5.3
4.2
13.3
13.7
9.7
12.3
12.9
12.1
16.6
13.8
M18
styrene
ppm
0.2
1.1
1.4
Volumrlflc
flow rate
dscfm
2001.0
1988.0
1989.3
3482.0
3511.0
3474.0
3489.0
3560.0
3530.0
3545.0
3545.0
Mass
Rate
Ib/hr
0.20
0.17
0.13
0.75
0.78
0.55
0.69
0.74
0.69
0.96
0.80
-------
Lasco - EPA
Conversion Summary Sheet
Condition ' Run
1 1
1 2
1 3
Average
2 1
2 2
2 3
Average
3 1
3 2
3 3
Average
4 1
4 2
4 3
Xwag*
5 1
5 2
5 3
Xwage
6 1
6 2
6 3
Average
7 1
7 2
7 3
Xverage
8 1
8 2
8 3
Average
9 1
10 1
11 1
25A
propane
ppm
43.5
41.7
39.5
41.6
43.5
38.1
34.6
38.7
185.7
189.1
204.7
193.2
231.0
226.6
NA
228.8
125.6
121.6
118.1
121.8
111.7
139.9
131.0
727.5
165.6
168.0
161.3
165.0
62.4
64.4
101.1
76.0
222.7
189.5
269.2
25A
propane
to carbon
PPm
130.5
125.1
118.5
124.7
130.5
114.3
103.8
116.2
557.1
567.3
614.1
579.5
693.0
679.8
NA
686.4
376.8
364.8
354.3
365.3
335.1
419.7
393.0
J82.6
496.8
504.0
483.9
494.9
187.2
193.2
303.3
227.9
668.1
568.5
807.6
GC
methane
ppm
83.1
91.2
87.0
87.1
81.4
77.0
85.0
81.1
50.1
49.4
48.7
49.4
55.3
58.9
NA
57.1
41.2
57.9
30.9
43.3
37.8
59.3
51.3
49.5
49.8
41.3
39.5
43.5
59.0
62.7
53.0
58.2
36.7
59.6
66.9
GC
methane
to carbon
ppm
83.1
91.2
87.0
87.7
81.4
77.0
85.0
81.1
50.1
49.4
48.7
49.4
55.3
58.9
NA
57.1
41.2
57.9
30.9
43.3
37.8
59.3
51.3
49.5
49.8
41.3
39.5
4J.5
59.0
62.7
53.0
58.2
36.7
59.6
66.9
GC
ethane
ppm
3.1
3.3
3.1
3.2
3.0
9.9
3.2
5.4
2.6
2.6
2.5
2.6
2.7
3.0
NA
2.9
1.8
2.2
1.3
1.8
1.6
2.3
1.9
1.9
1.9
1.6
1.6
1.7
2.9
2.8
2.7
2.8
1.5
2.5
2.9
GC
ethane
to carbon
ppm
6.2
6.6
6.2
6.3
6.0
19.8
6.4
10.7
5.2
5.2
5.0
5. 1
5.4
6.0
NA
5.7
3.6
4.4
2.6
J.5
3.2
4.6
3.8
3.9
3.8
3.2
3.2
3.4
5.8
5.6
5.4
5.6
3.0
5.0
5.8
Total
carbon
ppm
41.2
27.3
25.3
31.3
43.1
17.5
12.4
24. 3
501.8
512.7
560.4
525.0
632.3
614.9
NA
62 3. 6
332.0
3025
320.8
318.4
294.1
355.8
337.9
329.3
443.2
459.5
441.2
448.0
122.4
124.9
244.9
164.1
628.4
503.9
734.9
Total
propane
ppm
13.7
9.1
8.4
10.4
14.4
5.8
4.1
8.7
167.3
170.9
186.8
775.0
210.8
205.0
NA
207.9
110.7
100.8
106.9
106.1
98.0
118.6
112.6
109.8
147.7
153.2
147.1
749. 3
40.8
41.6
81.6
54.7
209.5
168.0
245.0
H2O
%
2.7
23
1.9
2.3
1.4
1.4
1.4
7.4
1.1
1.1
1.1
1.1
1.1
1.2
NA
7.2
2.5
2.5
2.5
2.5
2.3
2.1
1.9
2.7
1.3
1.3
1.3
...= '*L:3
1.3
3.1
4.9
3.1
4.5
0.2
0.3
Total
propane
dry
ppm
14.1
9.3
8.6
10.7
14.6
5.9
4.2
8.2
169.1
172.8
188.9
776.9
213.1
207.5
NA
210.3
113.5
103.4
109.7
1089
100.3
121.1
114.8
112.1
149.7
155.2
149.0
151.3
41.3
43.0
85.8
56.4
219.3
168.3
245.7
Response
factor
to
styrene
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
NA
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
Total
styrene
ppm
6.0
4.0
3.7
4.5
6.2
2.5
1.8
3.5
72.1
73.7
80.5
75.4
90.8
88.4
NA
89.6
48.4
44.1
46.8
46.4
42.8
51.6
48.9
47.8
63.8
66.2
63.5
64.5
17.6
18.3
36.6
24.1
93.5
71.7
104.7
M18
styrene
ppm
0.0
0.2
0.2
0.2
NA
23.6
22.7
34.1
7.2
48.6
18.9
Volumetric
flow rate
dscfm
1836.0
1893.0
1878.0
7869.0
1825.0
1769.0
1807.0
1800.3
1910.0
1852.0
1871.0
7S77. 7
1897.0
1850.0
NA
1873.5
1859.0
1890.0
1882.0
1877.0
1814.0
1835.0
1837.0
782S. 7
1746.0
1829.0
1833.0
1802.7
1918.0
1883.0
1854.0
1885.0
1763.0
1851.0
1872.0
Mass
Rate
Ib/hr
0.18
0.12
0.11
0.14
0.18
0.07
0.05
0.10
2.24
2.21
2.45
2.30
2.80
2.66
NA
2.7J
1.46
1.35
1.43
7.47
1.26
1.54
1.46
7.42
1.81
1.96
1.89
7.89
0.55
0.56
1.10
0.74
2.68
2.16
3.18
CONVSHT.XLS
-------
Lasco-EPA
Conversion Summary Sheet
Oven 10
Condition Run
II 2
11 3
Average
12 1
12 3
12 4
Average
13 1
13 -2
13 3
Average
25A
propane
ppm
283.6
273.3
275.4
240.9
280.5
284.3
265.6
331.8
340.3
334.0
335.4
25A
propane
to carbon
ppm
8S0.8
819.9
826.7
722.7
841.5
852.9
SOS. 7
995.4
1020.9
1002.0
1006.1
GC
methane
ppm
45.2
62.5
58.2
54.8
48.5
59.3
54.2
62.3
58.7
41.2
54.1
GC
methane
to carbon
ppm
45.2
62.5
5S.2
54.8
48.5
59.3
54.2
62.3
58.7
41.2
54.1
GC
ethane
ppm
1.9
2.5
2.4
2.8
2.5
3.1
2.8
3.2
3.0
2.1
2.8
GC
ethane
to carbon
ppm
3.8
5.0
4.9
5.6
5.0
6.2
5.6
6.4
6.0
4.2
5.5
Total
carbon
ppm
801.8
752.4
763.0
662.3
788.0
787.4
745.9
926.7
956.2
956.6
946.5
Total
propane
ppm
267.3
250.8
254. 3
220.8
262.7
262.5
24S.6
308.9
318.7
318.9
.J/5.5
H2O
%
0.5
1.2
0.7
0.5
1.6
2.7
1.6
2.2
2.2
2.2
2.2
Total
propane
dry
ppm
268.6
253.8
256.7
221.9
266.9
269.7
252.7
315.8
325.9
326.0
J22.6
Response
factor
to
styrene
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
Total
styrene
ppm
1 14.5
108.2
109.2
94.6
113.8
115.0
107.7
134.6
138.9
139.0
137.5
MIS
styrene
ppm
22.5
68.2
85.2
Volumtlrk
(low rate
dscfm
1823.0
1843.0
1846.0
1920.0
1842.0
1818.0
1860.0
1804.0
1823.0
1814.0
1813.7
Mass
Rate
Ib/hr
3.39
3.24
3.27
2.95
3.40
3.39
3.25
3.94
4.11
4.09
4.05
CONVSHT^S
-------
Lasco - EPA
Conversion Summary Sheet
Auxiliary Exhaust
Condition Run
5 1
5 2
5 3
Average
12 1
12 3
12 4
Average
13 1
13 2
13 3
Average
H20
%
2.1
2.1
2.1
2.1
1.7
1.6
1.6
1.6
1.6
1.7
1.7
1.7
Cone.
propane
wet
ppm
148.7
142.3
149.1
146.7
183.0
147.1
147.4
759.2
128.8
123.6
129.0
127.1
Cone.
propane
dry
ppm
151.9
145.4
152.3
149.8
186.2
149.5
149.8
161.8
130.9
125.7
131.2
129.3
Response
factor
to
styrene
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
Cone.
as
styrene
ppm
64.8
62.0
64.9
63.9
79.4
63.7
63.9
69.0
55.8
53.6
55.9
55.7
M18
styrene
ppm
34.5
49.0
40.0
30.5
Volumetric
flow rate
dscfm
4780.0
4677.0
4541.0
4666.0
4694.0
4731.0
4547.0
4657.3
4536.0
4471.0
4529.0
4512.0
Mass
Rate
!b/hr
5.02
4.70
4.79
4.84
6.05
4.89
4.71
5.22
4.11
3.89
4.11
4.04
CONVSHT.XLS
-------
Lasco - EPA
Conversion Summary Sheet
Main Exhaust
Condition Run
1 1
1 2
1 3
Average
2 1
2 2
2 3
Average
3 1
3 2
3 3
Average
4 I
4 2
4 3
Average
5 I
5 2
5 3
<4vefa#e
6 1
6 2
6 3
Average
7 1
7 2
7 3
/4vera#e
8 1
8 2
8 3
Average
9 I
10 I
11 1
11 2
11 3
Average
12 1
12 3
12 4
Average
13 1
13 2
13 3
Average
H2O
%
1.6
3.5
4.1
3.1
1.5
0.8
0.9
1.1
1.0
0.9
1.1
1.0
0.9
1.0
NA
1.0
2.0
2.1
2.4
2.2
2.2
2.3
1.9
2.1
1.8
1.5
1.4
1.6
1.2
1.5
1.5
1.4
1.6
1.4
1.4
1.7
1.6
1.6
1.7
1.6
1.1
1.5
1.4
1.7
1.9
1.7
Cone.
propane
wet
ppm
2965.4
2730.4
2798.6
2831.5
2553.6
2562.8
2378.0
2498.1
739.2
738.1
698.6
725.1
682.8
687.6
NA
655.2
476.0
426.9
413.5
438.8
861.0
868.0
877.6
868.9
717.5
859.4
876.6
817.8
612,8
622.3
667.9
634.3
609.3
600.9
547.5
558.3
561.2
5J5.7
368.0
313.5
304J
328.8
194.4
183.8
188.5
188,9
Cone.
propane
dry
ppm
3013.6
2829.4
2918.2
2921.0
2592.5
2583.5
2399.6
2525.1
746.7
744.8
706.4
732.6
689.0
694.5
NA
691.8
485.7
436.1
423.7
448.5
880.4
888.4
894.6
887.8
730.7
872.5
889.0
830.8
620.2
631.8
678.1
643.3
619.2
609.4
555.3
568.0
570.3
564.5
374.4
318.6
308.3
333.7
197.2
187.0
192.2
192.1
lesponse
factor
to
stvrene
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
NA
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
Cone.
as
styrene
ppm
1284.7
1206.2
1244.0
1245.0
1 105.2
1101.3
1022.9
1076.5
318.3
317.5
301.1
312.3
293.7
296.1
NA
294.9
207.1
185.9
180.6
191.2
375.3
378.7
381.4
378.5
311.5
371.9
379.0
354.1
264.4
269.3
289.1
274.3
264.0
259.8
236.7
242.1
243.1
240.7
159.6
135.8
131.4
142.3
84.0
79.7
81.9
81.9
MIS
styrene
ppm
673.9
510,9
189,4
176.0
129.2
171.6
NA
111,3
211.0
143.3
174.7
155.4
158,6
124.0
114.9
87.0
82.6
47.5
Volumetric
low rate
dscfm
3378.0
3030.0
2804.0
3070.7
3173.0
3105.0
3333.0
3203.7
3526.0
3414.0
3424.0
3454.7
3846.0
3823.0
NA
3834.5
3345.0
3314.0
3308.0
3322.3
3513.0
3449.0
3488.0
3483.3
3585.0
3593.0
3608.0
J59J.J
3724.0
3679.0
3661.0
3688.0
3624.0
3623.0
3672.0
3652.0
3581.0
3635.0
3459.0
3364.0
3305.0
3376.0
3362.0
3358.0
3325.0
3348.3
Mass
Rate
Ib/hr
70.44
59.32
56.62
62 .13
56.92
55.50 .
55.34 .
55.92
18.22
17.59
16.74
77.52
18.34
18.37
NA
18.35 .
11.24
10.00
9.70
10.31
21.40
21.20
21.59
21.40
18.12
21.69
22.20
20.67
15.98
16.08
17.18
16.41
15.53
15.28
14.11
14.35
14.13
14.20
8.96
7.42
7.05
7.81
4.59
4.34
4.42
4.45
CONVSHT.XLS
-------
Lasco - EPA
Conversion Summary Sheet
Room Exhaust
Condition Run
1 1
t 2
1 3
Average
2 I
2 2
2 3
Average
3 1
3 2
3 3
Average
4 1
4 2
4 3
Average
5 I
5 2
5 3
/Ive/afe
6 1
6 2
6 3
Average
7 1
7 2
7 3
<4vera£g
8 1
8 2
8 3
Average
9 I
10 1
11 t
11 2
11 3
Average
12 1
12 3
12 4
Average
13 1
13 2
13 3
Average
H2O
%
1.9
1.6
1.6
1.7
1.1
1.0
1.1
LI
0.8
0.9
0.8
0.8
0.9
0.9
NA
0.9
2.1
2.3
2.2
2,2
2.2
2.2
1.9
2.1
1.1
0.8
1.0
1.0
1.0
1.0
t.O
1.0
0.8
0.6
0,9
0.9
0.8
0.9
1.6
1.6
1.7
1.6
1.8
1.8
1.6
1,7
Cone.
iropane
wet
ppm
380.5
353.2
351.3
361.7
324.1
433.9
419.4
392.5
112.2
130.1
127.5
123.3
109.2
118.4
NA
U3.8
113.5
130.9
123.1
122.5
164.2
146.0
113.6
141.3
98.1
104.4
101.7
101.4
185.0
174.9
143.1
167.7
79.2
66.1
116.3
95.2
88.2
99.9
152.1
133.2
129.6
13S.3
100.3
104.5
106.9
103.9
Cone.
iropane
dry
ppm
387.9
358.9
357.0
367.9
327,7
438.3
424,1
396.7
113,1
131.3
128.5
124.3
110.2
119.5
Na
114,8
115.9
134.0
125.9
125.3
167.9-
149.3
115.8
144.3
99.2
105.2
102.7
102.4
186.9
176.7
144.5
169.4
79.8
66.5
117.4
96.1
88.9
100.8
154.6
135.4
131.8
140.6
102.1
106.4
108.6
105.7
Response
factor
to
styrene
0.4263
0.4263
0,4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
NA
0.4263
0,4263
0.4263
0,4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
0.4263
Cone.
as
styrene
ppm
165.3
153.0
152.2
/56.9
139.7
186.8
180.8
/69J
48.2
56,0
54.8
53.0
47.0
50.9
NA
49.0
49.4
57,1
53.7
53.4
71.6
63.6
49.4
61,5
42.3
44.9
43.8
43.6
79.7
75.3
61.6-
72.2
34.0
28.3
50.0
41.0
37.9
43.0
65.9
57.7
56.2
59,9
43.5
45.4
46.3
45.1
MIS
styrene
ppm
52.8
84.5
24.3
l.l
NA
29.6
37.1
14.5
37.9
21.0
5.5
18.0
8.4
23.1
low rate
dscfm
4886.0
4483.0
4644.0
4671.0
4637.0
4983.0
5062.0
4894.0
4961.0
4950.0
4974.0
4961.7
4846.0
4886.0
NA
4866.0
4402.0
4297.0
4619.0
4439.3
4663.0
4868.0
4920.0
4817.0
4772.0
4979.0
4753.0
4834.7
5144.0
5272.0
5013.0
5143.0
4728.0
4597.0
4694.0
4557.0
4863.0
4704,7
4541.0
4610.0
4350.0
4500.3
4465.0
4412.0
4447.0
4441.3
Mass
Rate
Ib/hr
13,11
11.13
11.47
11.91
10.51
15.11
14.85
13.49
3.88
4.50
4.42
4.27
3.69
4.04
NA
J.87
3.53
3.98
4.02
3.85
5.42
5.03
3.94
4.80
3.28
3.63
3.38
3.43
6.65
6.44
5.01
6.04
2.61
2.12
3.81
3.03
2.99
3.28
4.86
4.32
3.97
4.3S
3.16
3.25
3.34
3.25
GONVSHT.XLS
i -
-------
Lasco - EPa
NDO & Toial End. Mass rts.
Condition Run
1 1
1 2
1 3
Average
2 I
2 2
2 3
Average
3 1
3 2
3 3
Average
4 1
4 2
4 3
Average
5 I
5 2
5 3
Average
6 1
6 2
6 3
Average
1 \
1 2
7 3
Average
8 1
8 2
8 3
Average
Total NDO
Adj. Cone.
ppm, wet
6.5
6.5
6.5
6.5
11.6
11.6
11.6
77.6
10.8
10.8
10.8
MS
13.0
13.0
NA . -
13.0
2.1
2.1
2.1
2.1
3.4
3.4
3.4
3.4
2.3
2.3
2.3
2.3
7.5
7.5
7.5
7.5
Avgi
1120
%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
NA
7.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
1.9%
/.9%
Total NDO
Adj. Cone,
ppm, dry
6.6
6,6
6.6
6.6
11.8
11.8
11.8
11.8
11.1
11,1
11.1
11.1
13.3
13.3
NA
13.3
2.1
2.1
2.1
2.1
3.5
3.5
3.5
3.5
2.3
2.3
2.3
2.3
7.6
7.6
7.6
7.6
Total NDO
as Styrene
ppm
2.8
2.8
2.8
2.8
5.1
5.1
5.1
5J
4.7
4.7
4.7
4.7
5.1
5.7
NA
5.7
0.9
0.9
0.9
0.9
.5
.5
.5
1.5
.0
.0
.0
1.0
3.2
3.2
3.2
3.2
Total
Flow data
dscfm
8264.0
7513.0
7448.0
7741.7
7810.0
8088.0
8395.0
5097.7
8487.0
8364.0
8398.0
8416.3
8692.0
8709.0
NA
8700.5
12527.0
12288.0
12468.0
12427. 7
.8176.0
8317.0
8408.0
8300. 3
8357.0
8572.0
8361.0
8430.0
8868.0
8951.0
8674.0
8831.0
NDO
Mass rt.
Ib/hr, sty.
0.38
0.34
0.34
0.35
0.64
0.66
0.69
0.66
0.65
0.64
0.64
0.64
0.80
0.80
NA
0.80
0.18
0.18
0.18
0.18
0.20
0.20
0.20
0.20
0.14
0.14
0.14
0.14
0.47
0.47
0.46
0.47
M. Exhaus
Mass rt.
Ib/hr, sty.
70.44
59.32
56.62
62.13
56.92
55.50
55.34
55.92
18.22
17.59
16.74
77.52
18.34
18.37
NA
18.35
11.24
10.00
9.70
10.31
21.40
21.20
21.59
21.40
18.12
21.69
22.20
20.67
15.98
16.08
17.18
16.41
R. Exhaus
Mass rt.
Ib/hr, sty.
13.11
11.13
11.47
11.91
10.51
15.11
14,85
13.49
3.88
4.50
4.42
4.27
3.69
4.04
NA
3.87
3.53
3,98
4.02
155
5.42
5.03
3.94
4. 80
3.28
3.63
3.38
3.43
6.65
6.44
5.01
6.04
A. Exhaus
Mass rt.
Ib/hr, sty.
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
5.02
4.70
4.79
4.84
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Total Overall
Encl. Exhaust
Ib/hr, sty.
83.17
70.11
67.75
73.68
66.79
69.95
69.50
68. 75
21 .45
21.45
20.52
21. 14
21.23
21.61
NA
21.42
19.61
18.51
18.32
18.81
26.62
26.03
25.33
25.99
21.26
25.18
25.44
25.96
22.17
22.06
21.73
27.99
NDADAT^LS
-------
Lasco - EPa
al E
ass
Condition Run
9 1
10 1
11 1
11 2
11 3
Average
12 1
12 3
12 4
Average
13 1
13 2
13 3
Average
Total NDO
Adj. Cone.
ppm, wet
3.1
3.5
4.7
4.7
4.7
4.7
9.8
9.8
9.8
9.S
8.8
8.8
8.8
8.8
Avg.
H20
%
1.9%
1.9%
1.9%
1.9%
1.9%
/.9%
1.9%
1.9%
1.9%
7.9%
1.9%
1.9%
1.9%
7.9%
Total NDO
Adj. Cone.
ppm, dry
3.2
3.6
4.8
4.8
4.8
4.8
10.0
10.0
10.0
70.0
9.0
9.0
9.0
9.0
Total NDO
as Styrene
ppm
1.3
1.5
2.1
2.1
2.1
2.7
4.3
4.3
4.3
4.3
3.8
3.8
3.8
3.8
Total
Flow data
dscfm
8352.0
8220.0
8366.0
8209.0
8444.0
8339.7
12694.0
12705.0
12202.0
72533. 7
12363.0
12241.0
12301.0
12301.7
NDO
Mass rt.
Ib/hr, sty.
0.18
0.21
0.28
0.27
0.28
0.28
0.88
0.88
0.85
0.87
0.77
0.76
0.77
0.77
M. Exhaust
Mass rt.
Ib/hr, sty.
15.53
15.28
0.00
14.11
14.35
14.13
14.20
8.96
7.42
7.05
7.81
4.59
4.34
4.42
4.45
R. Exhaust
Mass rt.
Ib/hr, sty.
2.61
2.12
0.00
3.81
3.03
2.99
3.28
4.86
4.32
3.97
4. 38
3.16
3.25
3.34
3.25
A. Exhaust
Mass rt.
Ib/hr, sty.
NA
NA
NA
NA
NA
AM
6.05
4.89
4.71
5.22
4.11
3.89
4.11
4.04
Total Overall
Encl. Exhaust
Ib/hr, sty.
17.96
17.19
17.64
17.11
16.84
17.20
18.98
15.75
14.88
76.54
11.08
10.72
11.11
10.97
NDADATA.XLS
-------
Lasco - EPA
NDO Adjustments
Condition Run
1 1
2 1
3 1
4 1
5 1
6 1
7 1
8 1
9 1
10 1
11 1
12 1
13 1
flow
factor
0.84
0.82
0.81
0.82
0.87
0.84
0.83
0.78
0.78
0.79
0.77
0.86
0.85
NDO -A
Avg. Cone
ppm
6.0
13.4
12.8
15.6
2.3
3.4
2.4
8.3
3,2
3.8
5.6
11.3
10.1
Adj Cone
ppm
5.0
11.0
10.4
12.7
2.0
2.8
2.0
6.5
2.5
3.0
4.3
9.7
8.5
flow
factor
0.02
0.02
0.02
0.02
0.01
0.01
0.01
0.01
0.01
0.01
0.01
0.02
0.02
NDO-B
Avg. Con
ppm
6.0
4.4
7.5
1.6
1.3
14.1
2.9
2.5
2.7
2.6
1.8
0.6
2.9
Adj Cone
Ppm
0.1
0.1
0.2
0.0
0.0
0.1
0.0
0.0
0.0
0.0
0.0
0.0
0.0
flow -
factor
0.08
0.09
0.08
0.08
0.07
0.07
0.08
0.10
0.09
0.10
0.11
0.05
0.07
NDO-C
A'yg* Con
ppm
9.5
3.3
1.7
1.7
0.6
3.4
1.6
4.6
2.7
2.6
1.7
0.7
1.8
Adj Cone
ppm
0.7
0.3
0.1
0.1
0.0
0.2
0.1
0.5
0.2
0.3
0.2
0.0
0.1
flow
factor
0.07
0.08
0.09
0.08
0.05
0.08
0.09
0.11
0.12
0.10
0.11
0.07
0.07
NDO-D
Avg. Con
ppm
9.5
3.3
1.7
1.7
0.6
3.4
1.6
4.6
2.7
2.6
1.7
0.7
1.8
Adj Cone
ppm
0.6
0.3
0.1
0.1
0.0
0.3
0.1
0.5
0.3
0.3
0.2
0.1
0.1
Total NDO
Adj. Cone.
ppm, wet
6.5
11.6
10.8
13.0
2.1
3.4
2.3
7.5
3.1
3.5
4.7
9.8
8.8
NDADAT.
-------
Flo
Condition Run
1 1
1 2
1 3
Average
2 1
2 2
2 3
Average
3 1
3 2
3 3
,4 wage
4 1
4 2
4 3
Average
5 1
5 2
5 3
/Iverage
6 1
6 2
6 3
Average
7 1
7 2
7 3
Average
8 1
8 2
8 3
Average
flow
fpm
275.0
235.0
230.0
246.7
225.0
235.0
225,0
228.3
225.0
240.0
230.0
231.7
250.0
275.0
NA
262.5
325.Q
325.0
325.0
325.0
300.0
250.0
275.0
275.0
250.0
250.0
300.0
266.7
275.0
300.0
300.0
291.7
NDO-A
rate
cfm
7334.0
6267.0
6134.0
6578.3
6000.0
6267,0
6000.0
6089.0
6000.0
6400.0
6134.0
6178.0
6668.0
7334.0
NA
7001.0
8668.0
8668.0
8668.0
8668.0
8001.0
6668.0
7334.0
7334.3
6668.0
6668.0
8001.0
7112.3
7334.0
8001.0
8001.0
7778.7
Cone.
ppra
6.1
5.0
6.9
6.0
5.7
4.5
30.1
13.4
12.0
15.1
11,3
12.8
12.8
18.3
NA
75.6
1.1
4.7
1.1
2.3
3.9
3.8
2.4
3.4
3.4
2.0
1.9
2.4
11.0
5.6
NA
8.3
flow
fpm
550.0
600.0
600.0
583.3
450.0
350.0
550.0
¥50.0
650.0
650.0
650.0
650.0
700.0
700.0
NA
700.0
500.0
400.0
500.0
466.7
250.0
250.0
200.0
233.3
200.0
200.0
300.0
233.3
550.0
400.0
400.0
450.0
NDO-B
rate
cfm
138.0
150.0
150.0
146.0
113.0
88.0
138.0
113.0
163.0
163.0
163.0
163.0
175.0
175.0
NA
/75.0
125-0
100.0
125.0
116.7
62.5
62.5
50.0
58.3
50.0
50.0
75.0
58.3
138.0
100.0
100.0
112.7
Cone,
ppm
NA
6.0
6.0
6.0
NA
NA
4.4
4.4
12.3
1.8
8.3
7.5
1.6
NA
NA
1.6
0.0
0.5
3.3
1.3
3.0
9.7
29.6
14.1
3.5
3.8
1.4
2.9
NA
2.5
NA
2.5
flow
fpm
263.0
230.0
240.0
244. 3
265-0
260.0
260.0
261,7
245,0
240.0
240.0
241.7
250.0
300.0
NA
275.0
300.0
275.0
275.0
283.3
250.0
250.0
250.0
250.0
250.0
250.0
300.0
266.7
550.0
350.0
300.0
400.0
NDO-C
rate
cfm
665.0
582.0
607.0
618.0
670.0
658.0
658.0
662.0
620.0
607.0
607.0
611.3
633.0
759.0
NA
696.0
759.0
696.0
696.0
717.0
633.0
633.0
633.0
6JJ.O
633.0
633.0
759.0
675.0
1392.0
886.0
759.0
1012.3
Cone.
ppm
15.9
NA
3.0
9.5
1.6
2.9
5.4
3.3
0.6
1.8
2.8
1.7
1.7
1.6
NA
1.7
0.0
0.9
0.8
0.6
2.7
5.6
1.9
3.4
2.2
1.5
1.0
1.6
6.2
3.0
NA
4.6
flow
fpm
210.0
200.0
200.0
203. 3
200.0
210.0
260.0
223.3
260.0
250.0
260.0
256.7
275.0
275.0
NA
275.0
210.0
200,0
200.0
20J.J
250.0
250.0
350.0
283. 3
300.0
300.0
300.0
300.0
450,0
400.0
400.0
416.7
NBO-D
rate
cfm
531.0
506.0
506.0
514.3
506.0
531.0
658.0
565.0
658.0
633.0
658.0
649.7
696.0
696.0
NA
696.0
531.0
506.0
506.0
514.3
633.0
633.0
886.0
717.3
759.0
759.0
759.0
759.0
1139.0
1012.0
1012.0
1054.3
Cone.
ppm
15.9
NA
3.0
9.5
1.6
2.9
5.4
3.3
0.6
1.8
2.8
1.7
1.7
1.6
NA
1.7
0.0
0.9
0.8
0.6
2.7
5.6
1.9
3.4
2.2
1.5
1.0
1.6
6.2
3.0
NA
4.6
NDADATA.XLS
-------
Lasco - EPA
NDO Flow Data
Condition Run
9 1
10 1
11 1
11 2
11 3
Average
12 1
12 3
12 4
Average
13 1
13 2
13 3
^vcrage
flow
fpm
250.0
300.0
300.0
300.0
200.0
266.7
450.0
450.0
450.0
450.0
450.0
450.0
450.0
450.0
NDO -A
rate
cfm
6668.0
8001.0
8001.0
8001.0
5334.0
7112.0
12002.0
12002.0
12002.0
12002.0
12002.0
12002.0
12002.0
12002.0
Cone.
ppm
3.2
3.8
8.0
5.0
3.9
5.6
10.8
12.0
11.2
11.3
11.7
10.1
8.4
10.1
flow
fpm
300.0
550.0
525.0
525.0
525.0
525.0
1000.0
950.0
850.0
933.3
950.0
950.0
950.0
950.0
NDO-B
rate
cfm
75.0
138.0
131.0
131.0
131.0
131.0
250.0
238.0
213.0
233.7
238.0
238.0
238.0
238.0
Cone.
ppm
2.7
2.6
1.5
0.9
3.1
1.8
1.4
0.2
0.2
0.6
4.2
1.5
3.1
2.9
flow
fpm
300.0
400.0
400.0
400.0
400.0
400.0
250.0
300.0
300.0
283.3
300.0
400.0
400.0
366.7
NDO-C
rate
cfm
759.0
1012.0
1012.0
1012.0
1012.0
1012.0
633.0
759.0
759.0
717.0
759.0
1012.0.
1012.0
927.7
Cone.
ppm
2.7
2.6
3.3
1.0
0.8
1.7
1.5
0.3
0.4
0.7
1.8
1.9
1.8
1.8
flow
fpm
400.0
400.0
400.0
400.0
400.0
400.0
350.0
450.0
400.0
400.0
400.0
400.0
400.0
400.0
NDO-D
rate
cfm
1012.0
1012.0
1012.0
1012.0
1012.0
1012.0
886.0
1139.0
1012.0
1012.3
1012.0
1012.0
1012.0
1012.0
Cone.
ppm
2.70
2.60
3.30
1.00
0.78
1.7
1.5
0.3
0.4
0.7
1.8
1.9
1.8
1.8
NDADATA-XLS
-------
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PACIFIC ENVIRONMENTAL SERVICES, INC.
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Condition 1 Method 18 Sampling Results
Y =
Pressure ,„„,„„«
Vacuum maer
TemperaturemeUT
ME-1-3
Initial volume
Final Volume
Volume
5Undln,
0.997
28.92 inches of mercury
0.0 inches of mercury
71 ° Fahrenheit
2268.33 Liters
2274.54 Liters
6.21 Liters
5.71 Liters
Charcoal tube sample Styrene concentration = Mass Liqili<1
Volume sundart
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 2
Start Time 15:40
Finish Time 16:05
Moisture 4.1 %
Mass Li^ 16.66 Milligrams
2.9194 mg/liter
673.9 ppm
Pressure bironiaric
Vacuum mno
RE-1-3 Initial volume
Final Volume
Volume™^
0.999
28.92 inches of mercury
0.0 inches of mercury
74 ° Fahrenheit
7664.32 Liters
7678.92 Liters
14.60 Liters
Volume 5Undln, 13.72 Liters
Charcoal tube sample Styrene concentration = Mass Liquid
Volume sun(laiTl
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
; r.- Meter VOST 1
'Start Time 15:41
Finish Time 16:41
Moisture 1.6%
Mass Uquid 3.14 Milligrams
0.2289 mg/liter
52.8 ppm
Y
Pressure
Vacuum
Temperature,
9-1-2
Initial volume
Final Volume
Volume
1.052
28.92 inches of mercury
0.0 inches of mercury
91 ° Fahrenheit
849.80 Liters
865.59 Liters
15.79 Liters
15.11 Liters
Meter ES-1
Start Time 12:35
Finish Time 13:35
Moisture 1.8%
Charcoal tube sample Styrene concentration =
Mass
Volume
Concentration, pan per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
XXXX Milligrams
= ######## mg/liter
= ######## ppm
Pagel
-------
Condition 1 Method 18 Sampling Results
Y =
Pressure ta^nanc
Vacuum maa
Temperaturemeler
10-1-1 Initial volume
Final Volume
Volumemaer
1.052
28.80 inches of mercury
0.0 inches of mercury
84 ° Fahrenheit
834.18 Liters
849.68 Liters
15.50 Liters
Volume sundinl • 14.82 Liters
Charcoal tube sample Styrene concentration = Mass Liquid
Concentration, part per million (ppm)
Volume slandinl
ug/liter x 24.04 liter/mole
molecular weight
Meter ES-1
Start Time 10:40
Finish Time 11:40
Moisture 2.7%
Mass Liquid 0.00 Milligrams
0.0001 mg/liter <
= 0.0 ppm
Y =
Pressure bitomaiic
Vacuum mner
Temperaturemaer
NDA-1-1 Initial Volume
Final Volume
1.017
28.92 inches of mercury .
2.0 inches of mercury
85 ° Fahrenheit
1306,74 Liters
1329.30 Liters
22.56 Liters
Volume 5Undlrt 21.27 Liters
Charcoal tube sample Styrene concentration =
Meter VOST 3
Start Time 10:35
Finish Time 11:35
Moisture 1.0%
Mass Ii()llid
Mass Liquid
Volume
sandlld
Concentration, part per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
0.01 Milligrams
0.0005 mg/liter
0.1 ppm
Y - 1.017
Pressure bawnaric 28.80 inches of mercury Meter
Vacuum „,„, 1 .0 inches of mercury Start Time
Temperaturemoj, 88.4 ° Fahrenheit Finish Time
NDB-1-3 Initial volume 1321.34
Final Volume 1337.08
Volume^ 15.74
Volume smM 14.70
Charcoal tube sample Styrene concentration
Concentration, pan per million (ppm) =
Liters Moisture
Liters
Liters
Liters Mass uquki
= MaSS Ljquid =
Volume jama*
ug/liter x 24.04 liter/mole =
molecular weight
VOST3
15:40
16:40
0.9%
0.00 Milligrams
0.0001 mg/liter
0.0 ppm
Page 2
-------
Condition 2 Method 18 Sampling Results
Pressure taroni0nc
Vacuum maa
Temperaturemoet
ME-2-1
Initial Volume
Final Volume
Volume,^
Volume
suniunl
0.997
28.84 inches of mercury
1.0 inches of mercury
69 ° Fahrenheit
2275.08 Liters
2283.95 Liters
8.87 Liters
8.38 Liters
Meter VOST 2
Start Time 20:23
Finish Time 20:54
Moisture 1.5%
Mass
Charcoal tube sample Styrene concentration = Mass Uquid
Volume
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
18.55 Milligrams
2.2135 mg/liter
510.9 ppm
Y =
Pressure
Vacuum
Temperature,
RE-2-1
0.999
28.84 inches of mercury
1.0 inches of mercury
71 ° Fahrenheit
7679.50 Liters
7694.21 Liters
14.71 Liters
Volume sundart 13.93 Liters
Charcoal tube sample Styrene concentration =
Initial Volume
Final Volume
Mass
Liquid
Volume
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 1
Start Time 20:20
Finish Time 21:22
Moisture 1.1%
Mass Liqui<1 5.1 Milligrams
0.3661 mg/liter
= 84.5 ppm
Pressure
Vacuum
Temperaturcnaj,
9-2-1
1.052
28.92 inches of mercury
0.0 inches of mercury
85 ° Fahrenheit
866.91 Liters
881.20 Liters
14.29 Liters
13.89 Liters
Charcoal tube sample Styrene concentration
Initial Volume
Final Volume
Meter ES-1
Start Time 17:35
Finish Time 18:38
Moisture 1.3%
Volume
Mass
Volume
„,„,,„,
Concentration, pan per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
0.02 Milligrams
0.0014 mg/liter
0.3 ppm
-------
Condition 2 Method 18 Sampling Results
Y = 1.052
Pressure baroinaiic 28.80 inches of mercury
Vacuum maet 0.0 inches of mercury
TemperaturemelCT 87 ° Fahrenheit
10-2-2 Initial Volume 881.65 Liters
Final Volume 897.00 Liters
Volume,™^ 15.35 Liters
Volume nandard 14.78 Liters
Charcoal tube sample Styrene concentration = Mass Liquid
Volume sundjrf
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter ES-1
Start Time 22:00
Finish Time 23:00
Moisture 1.5%
Detection Limit
Mass Liquid 0-01 Milligrams
0.0007 mg/liter
= 0.2 ppm
Y = 1.017
Pressure h,rraneuic 28.84 inches of mercury
Vacuum meler 1 .0 inches of mercury
TemperaturCme^, 87 ° Fahrenheit
NDA-2-2 Initial Volume 1337.15 Liters
Final Volume 1 35 1 . 8 1 Liters
VolumCjnaCT 14.66 Liters
Volume Handird 13.73 Liters
Charcoal tube sample Styrene concentration = Mass | iquid
Volume sundari
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
Meter VOST 3
Start Time 22:00
Finish Time 23:00
Moisture 1.0%
Mass u,uid 0-05 Milligrams
0.0036 mg/liter
= 0.8 ppm
molecular weight
Y = 1.017
Pressure tammanc 28.84. inches of mercury
Vacuum maer 1.0 inches of mercury
TemperaturCroaj, 92 ° Fahrenheit
NDB-2-3 Initial Volume 1352.10 Liters
Final Volume 1366.82 Liters
Volume^,., 14.72 Liters
Volume .aatari 13.65 Liters
Charcoal tube sample Styrene concentration = Mass Liquid
Volume janujri
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
Meter VOST 3
Start Time 23:30
Finish Time 0:30
Moisture 1.1%
Mass Liquid °-01 Milligrams
0.0007 rag/liter
= 0.2 ppm
molecular weight
-------
Condition 3 Method 18 Sampling Results
Y = 0.997
Pressure barometric 28.90 inches of mercury Meter
Vacuum „,„„ 1 .0 inches of mercury Start Time
TemperaturemttCT 64 ° Fahrenheit Finish Time
ME-3-1 Initial Volume
Final Volume
VolumemMr
Volume sttau,,,,
2287.47 Liters Moisture
2290.49 Liters
3.02 Liters
2.90 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass \ iquid =
Concentration, pan per million
Volume stin(tard
(ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST2
14:25
14:55
1.0%
2.38 Milligrams
0.8204 mg/liter
189.4 ppm
Y » 0.997
Pressure tsmaanc 28.90 inches of mercury
Vacuum maa 1.0 inches of mercury
58 ° Fahrenheit
ME-3-2 Initial Volume 2290.74 Liters
2292.91 Liters
2.17 Liters
2.11 Liters
Initial Volume
Final Volume
VolumemMr
Volume
Meter VOST2
Start Time 16:00
Finish Time 16:20
Moisture 0.9%
Mass
Charcoal tube sample Styrene concentration = Mass i.i<|ua
Volume sundlnl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
1.61 Milligrams
0.7627 mg/liter
176.0 ppm
ME-3-3
Pressure
Vacuum „„„
Temperaturen.ae,
Initial Volume
Final Volume
Volume
0.997
29.10 inches of mercury
1.0 inches of mercury
57 ° Fahrenheit
2293.37 Liters
2294.61 Liters
1.24 Liters
1.21 Liters
Meter VOST2
Start Time 17:35
Finish Time 17:50
Moisture 1.1%
Mass
Charcoal tube sample Styrene concentration
Concentration, pan per million (ppm)
Mass
Volume
ug/liter x 24.04 liter/mole
molecular weight
0.68 Milligrams
0.5599 mg/liter
129.2 ppm
Pagel
-------
Condition 3 Method 18 Sampling Results
Y = 0.999
Pressure barometric 28.90 inches of mercury Meter
Vacuum maer 1.0 inches of mercury Start Time
Temperaturemaer 60 ° Fahrenheit Finish Time
RE-3-1 Initial Volume 7694.32 Liters Moisture
Final Volume 7706.45 Liters
VolumemHCT 12.13 Liters
Volume sundlnl 11.79 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume sundini
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 1
14:25
15:25
0.8%
1.24 Milligrams
0.1052 mg/liter
24.3 ppm
Y = 1.052
Pressure ^romanc 28.90 inches of mercury Meter
Vacuum maa 0.0 inches of mercury Start Time
TemperaturCraae, 86 ° Fahrenheit Finish Time
9-3-2 Initial Volume 912.12 Liters Moisture
Final Volume 926.48 Liters
VolumemaCT 14.36 Liters
Volume 5Undlrt 13.96 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Uquid =
Volume sundini
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
16:00
17:00
1.1%
0.05 Milligrams
0.0036 mg/liter
0.8 ppm
Y =
Pressure
Vacuum
Temperature,
10-3-1
Initial Volume
Final Volume
1.052
28.90 inches of mercury
0.0 inches of mercury
82 ° Fahrenheit
897.24 Liters
911.91 Liters
14.67 Liters
Meter ES-1
Stan Time 14:25
Finish Time 15:25
Moisture 1.1%
Volume jaildirt 14.36 Liters
Charcoal tube sample Styrene concentration =
Mass u
Mass
Volume
Concentration, pan per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
Detection Limit
0.01 Milligrams
0.0007 mg/liter
0.2 ppm
Page 2
-------
Condition 3 Method 18 Sampling Results
Y =
Pressure buomaric
Vacuum moer
Temperaturemoer
NDA-3-2 Initial Volume
Final Volume
1.017
29.10 inches of mercury
1.0 inches of mercury
87 ° Fahrenheit
1367.17 Liters
1382.08 Liters
14.91 Liters
Volume Janata 14.11 Liters
Charcoal tube sample Styrene concentration = Mass Liqmd
Meter VOST 3
Start Time 15:57
Finish Time 16:49
Moisture 0.9%
Mass
Liquid
Volume sundanl
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.09 Milligrams
0.0064 mg/liter
1.5 ppm
Y = 1.017
Pressure blroinoiic 29.10 inches of mercury Meter
Vacuum maa 1 .0 inches of mercury Start Time
Temperature^^ 93 ° Fahrenheit Finish Time
NDB-3-3 Initial Volume
Final Volume
Volume,^
Volume sun
-------
Condition 4 Method 18 Sampling Results
Pressure barometric
Vacuum maa
Temperaturemr[er
ME-4-2 Initial Volume
Final Volume
Volumemaer
0.997
29.20 inches of mercury
1.0 inches of mercury
51 "Fahrenheit
2296.54 Liters
2298.54 Liters
2.00 Liters
Meter VOST 2
Start Time 21:30
Finish Time 21:45
Moisture 1.0%
Volume 5UDlUri 1.99 Liters
Charcoal tube sample Styrene concentration =
Mass Uqilid
Mass
( iquid
Volume
sunitari
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
1.48 Milligrams
0.7435 mg/liter ,
171.6 ppm
Y = 0.997
Pressure barometric 29.20 inches of mercury Meter
Vacuum „„„ 1 .0 inches of mercury Start Time
TemperaturemaCT 55 ° Fahrenheit Finish Time
RE-4-1 Initial Volume
Final Volume
Volume,,^
Volume sunltart
Charcoal tube sample Styrene
2294.61 Liters Moisture
2296.43 Liters
1.82 Liters
1.80 Liters Mass Uquid
concentration = Mass { iquid =
Volume sunitari
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 2
20:05
20:20
0.9%
0.08 Milligrams
0.0444 mg/liter
10.3 ppm
Y = 1.052
Pressure taromaro 28.80 inches of mercury Meter
Vacuum „„., 0.0 inches of mercury Start Time
Temperature,,^ 90 ° Fahrenheit Finish Time
9-4-2 Initial Volume 941.12 Liters Moisture
Final Volume 956.55 Liters
Volume,,.^ 15.43 Liters
Volume TOPH.^ 14.82 Liters Mass ^^
Charcoal tube sample Styrene concentration = Mass uquid —
Volume jnafcnj
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
21:40
22:30
1.2%
0.77 Milligrams
O.OS20 mg/liter
12.0 ppm
Pagel
-------
Condition 4 Method 18 Sampling Results
Pressure
Vacuum
10-4-1
Initial Volume
Final Volume
Volume™^
1.052
28.90 inches of mercury
0.0 inches of mercury
84 ° Fahrenheit
926.56 Liters
941.10 Liters
14.54 Liters
Meter ES-1
Stan Time 20:05
Finish Time 21:05
Moisture 1.1%
Volume jundiid 14.18 Liters
Charcoal tube sample Styrene concentration = Mass Liqu,d
Mass
Volume j
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Detection Limit
0.01 Milligrams
0.0007 mg/liter
0.2 ppm
Pressure
Vacuum
NDA-4-1 Initial Volume
Final Volume
Volume,^
1.017
28.80 inches of mercury
1.0 inches of mercury
90 ° Fahrenheit
1399.28 Liters
1413.68 Liters
14.40 Liters
Meter VOST3
Stan Time' V20:05
Finish Time 21:05
Moisture 1.0%
Volume tuatart 13.40 Liters
Charcoal tube sample Styrene concentration =
Mass
Mass
Liquid
Volume
Concentration, pan per million (ppm) =
ug/liter x 24.04 liter/mole
molecular weight
0.09 Milligrams
0.0067 mg/liter
= 1.6 ppm
Pressure baraomk
Vacuum
NDB-4-2 Initial Volume
Final Volume
Volume
1.017
29.20 inches of mercury
1.0 inches of mercury
92 ° Fahrenheit
1413.94 Liters
1429.57 Liters
15.63 Liters
14.68 Liters
Meter VOST3
Start Time 21:30
Finish Time 22:30
Moisture 1.1%
Mass
Charcoal tube sample Styrene concentration
Concentration, part per million (ppm)
Mass
Uquid
Volume
ug/liter x 24.04 liter/mole
molecular weight
Detection Limit
0.01 Milligrams
0.0007 mg/liter
0.2 ppm
Page 2
-------
Condition 5 Method 18 Sampling Results
Y =
Pressure baroniaric
Vacuum mBCT
Temperaturemeter
ME-5-1 Initial Volume
Final Volume
Volume,,,^
0.997
28.85 inches of mercury
1.0 inches of mercury
75 ° Fahrenheit
2298.73 Liters
2300.27 Liters
1.54 Liters
Meter VOST2
Start Time 9:05
Finish Time 9:20
Moisture 2.1%
Volume SUIXtanj 1.43 Liters
Charcoal tube sample Styrene concentration = Mass Liqui(i
MaSS Liquid
Volume sun(tard
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.69 Milligrams
0.4824 mg/liter
111.3 ppm
Y =
Pressure haromnhc
Vacuum maer
TemperaturemBCT
RE-5-1
Initial Volume
Final Volume
Volume,^
0.999
28.85 inches-of mercury
1.0 inches of mercury
79 ° Fahrenheit
7713.90 Liters
7720.65 Liters
6.75 Liters
Volume sundlrt 6.24 Liters
Charcoal tube sample Styrene concentration
Mass Liquid
Meter VOST 1
Start Time 9:04
Finish Time 9:49
Moisture 2.1%
Detection Limit
Mass Liquid °-80 Milligrams
0.1283 mg/liter
Volume
sundird
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
^ molecular weight
29.6 ppm
Pressure
Vacuum „„„
Temperaturen^
AF-5-2
Initial Volume
Final Volume
Volume
0.999
28.80 inches of mercury
1.0 inches of mercury
93 ° Fahrenheit
7721.07 Liters
7728.80 Liters
7.73 Liters
6.95 Liters
Meter VOST 1
Stan Time 11:08
Finish Time 12:08
Moisture 2.1%
Mass
Charcoal tube sample Styrene concentration
Concentration, pan per million (ppm)
Mass
Volume
ug/liter x 24.04 liter/mole
molecular weight
1.04 Milligrams
= 0.1497 mg/liter
= 34.5 ppm
Pagel
-------
Condition 5 Method 18 Sampling Results
9-5-1
Pressure b>roniaric
Vacuum maa
Temperaturemeter
Initial Volume
Final Volume
Volume
5Undlu1j
1.052
29.25 inches of mercury
0.0 inches of mercury
82 ° Fahrenheit
957.55 Liters
972.61 Liters
15.06 Liters
14.67 Liters
Meter ES-1
Start Time 9:04
Finish Time 10:04
Moisture 2.8%
Mass Uquid
Mass Liquid
Volume j
Charcoal tube sample Styrene concentration =
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.09 Milligrams
0.0061 mg/liter
1.4 ppm
Y =
Pressure hironwhc
Vacuum maa
Temperature,^
10-5-2 Initial Volume
Final Volume
Volumemaer
Volume iundlld
1.052
29.25 inches of mercury Meter
0.0 inches of mercury Start Time
91 ° Fahrenheit Finish Time
972.65 Liters Moisture
987.82 Liters
15.17 Liters
14.58 Liters Mass Uquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume sundlld
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
11:08
12:08
2.5%
1.49 Milligrams
0.1022 mg/liter
23.6 ppm
Pressure „,„„,„«
Vacuum „„„
Temperature.^
NDA-5-1 Initial Volume
Final Volume
Volume
1.017
28.85 inches of mercury
1.0 inches of mercury
84 ° Fahrenheit
1429.79 Liters
1445.29 Liters
15.50 Liters
14.44 Liters
Meter VOST 3
Start Time 9:02
Finish Time 10:02
Moisture 2.1%
Mass
Charcoal tube sample Styrene concentration
Mass
Volume
Concentration, pan per million (ppm) =
ug/liter x 24.04 liter/mole
molecular weight
Detection Limit
0.01 Milligrams
0.0007 mg/liter
0.2 ppm
Page 2
-------
Condition 5 Method 18 Sampling Results
Y = 1.017
Pressure baoaxttic 28.80 inches of mercury •
Vacuum mHer 1.0 inches of mercury
TemperaruremnCT 97 ° Fahrenheit
NDB-5-2 Initial Volume
Final Volume
Volumemner
Volume sundird
1445.42 Liters
1459.99 Liters
14.57 Liters
13.39 Liters
Charcoal tube sample Styrene concentration = Mass Liquid
Concentration, pan per million
Volume 5Undard
(ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 3
Stan Time 11:08
Finish Time 12:08
Moisture 1.0%
Detection Limit
Mass Liquid 0.01 Milligrams
0.0007 mg/iiter
0.2 ppm
Page 3
-------
Condition 6 Method 18 Sampling Results
Y = 0.997
Pressure ^00^^ 28.78
Vacuum maa 1.0
Temperaturemcler 78
ME-6-2 Initial Volume
Final Volume
Volumemcler
Volume sun(tan,
inches of mercury Meter
inches of mercury Stan Time
0 Fahrenheit Finish Time
2308.46 Liters Moisture
2310.28 Liters
1.82 Liters
1.67 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume SUIldart
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST2
17:33
17:43
2.3%
1.53 Milligrams
0.9142 mg/liter
21 1.0 ppm
Y = 0.999
Pressure haronielric 28.78
Vacuum mner 1 .0
Temperature,^ 86
RE-6-1 Initial Volume
Final Volume
Volumemaer
Volume sundinl
inches of mercury Meter
inches of mercury Stan Time
0 Fahrenheit Finish Time
7729.04 Liters Moisture
7735.75 Liters
6.71 Liters
6. 10 Liters Mass L^
Charcoal tube sample Styrene concentration = Mass Uquid =
Volume SUIIdird
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 1
16:06
16:51
2.2%
0.98 Milligrams
0. 1607 mg/liter
37.1 ppm
Y = 1.052
Pressure („,„„,« 29.20 inches of mercury Meter
Vacuum „,„, 0.0 inches of mercury Stan Time
Temperature^a, 96 ° Fahrenheit Finish Time
9-6-2 Initial Volume 1001.46
Final Volume 1016.29
Volumeinaer 14.83
Volume jaafcrt 14.14
Charcoal tube sample Styrene concentration
Concentration, pan per million (ppm) =
Liters Moisture
Liters
Liters
Liters Mass Liquid
= MaSS [j^ =
Volume stndiri
ug/liter x 24.04 liter/mole =
molecular weight
ES-1
17:33
18:33
2.2%
0.09 Milligrams
0.0064 mg/liter
1.5 ppm
Pagel
-------
Condition 6 Method 18 Sampling Results
Y = 1.052
Pressure barometric 29.20 inches of mercury Meter
Vacuum mBer 0.0 inches of mercury Start Time
TemperaturemBCT 93 ° Fahrenheit Finish Time
10-6-1 Initial Volume 987.85 Liters Moisture
Final Volume 1001.42 Liters
Volumemner 13.57 Liters
Volume sundari 13.00 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Uquid =
Volume sunitart
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
16:05
16:58
2.3%
1.28 Milligrams
0.0985 mg/liter
22.7 ppm
Y = 1.017
Pressure baromanc 28.78 inches of mercury Meter
Vacuum maa 1 .0 inches of mercury Start Time
TemperaturemBef 97 ° Fahrenheit Finish Time
NDA-6-1 Initial Volume 1460.09 Liters Moisture
Final Volume 1475.64 Liters
Volume^,,, 15.55 Liters
Volume sunitart 14.10 Liters Mass Uquid
Charcoal tube sample Styrene concentration = Mass Uquid =
Volume sunitart
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 3
16:05
17:05
2.2%
0.02 Milligrams
0.0014 mg/liter
0.3 ppm
Y = 1.017
Pressure (aroma™ 28.84 inches of mercury Meter
Vacuum maa 1 .0 inches of mercury Stan Time
Temperaturengu, 90 ° Fahrenheit Finish Time
NDA-6-3 Initial Volume 1475.69 Liters Moisture
Final Volume 1485.63 Liters
VoiumeQae, 9.94 Liters
Volume nanhn, 9.18 Liters Massu^
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume jonbrt
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 3
19:37
20:17
1.9%
Detection Limit
0.01 Milligrams
0.0011 mg/liter
0.3 ppm
Page 2
-------
Condition 7 Method 18 Sampling Results
Y = 0.997
Pressure taronttuic 28.92
Vacuum maa 1.0
TemperaturemBer 77
ME-7-1 Initial Volume
Final Volume
Volumema£r
Volume sundlld
inches of mercury Meter
inches of mercury Stan Time
0 Fahrenheit Finish Time
2310.34 Liters Moisture
2312.66 Liters
2.32 Liters
2.16 Liters Mass Uquid
Charcoal rube sample Styrene concentration = Mass Liquid =
Volume SQndinl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST2
14:49
15:04
1.8%
1.34 Milligrams
0.6207 mg/liter
143.3 ppm
Y = 0.997
Pressure h,™^ 28.92
Vacuum maer 1.0
Temperature^^, 66
ME-7-3 Initial Volume
Final Volume
Volume snnd.rt
inches of mercury Meter
inches of mercury Stan Time
0 Fahrenheit Finish Time
2312.80 Liters Moisture
2315.10 Liters
2.30 Liters
2.19 Liters Mass Uquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume sundinl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST2
19:13
19:28
1.4%
1.66 Milligrams
0.7567 mg/liter
174.7 ppm
Y =
Pressure
Vacuum
Temperature,
RE-7-1
Initial Volume
Final Volume
Volume
0.999
28.92 inches of mercury
1.0 inches of mercury
71 ° Fahrenheit
7737.46 Liters
7741.65 Liters
4.19 Liters
3.98 Liters
Meter VOST 1
Stan Time 14:49
Finish Time 15:19
Moisture 1.1%
Mass
Charcoal tube sample Styrene concentration
Concentration, part per million (ppm)
Mass
Volume
ug/liter x 24.04 liter/mole
molecular weight
0.25 Milligrams
0.0628 mg/liter
14.5 ppm
Pagel
-------
Condition 7 Method 18 Sampling Results
Y =
Pressure barometric
Vacuum mner
Temperaturemner
9-7-1
Initial Volume
Final Volume
Volume,,,^
1.052
28.92 inches of mercury
0.0 inches of mercury
92 ° Fahrenheit
16.32 Liters
28.13 Liters
11.81 Liters
Volume sundard 11.35 Liters
Charcoal rube sample Styrene concentration =
Mass , iquid
Meter ES-1
Start Time 14:49
Finish Time 15:49
Moisture 1.2%
Detection Limit
Mass Liquid 0.01 Milligrams
0.0009 mg/liter
Volume
Concentration, pan per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
0.2 ppm
Y =
Pressure haromonc <
Vacuum maet
Temperature,^
10-7-2 Initial Volume
Final Volume
Volume,™,,,
Volume suatard
1.052
28.92 inches of mercury Meter
0.0 inches of mercury Stan Time
90 ° Fahrenheit Finish Time
28.15 Liters Moisture
43.62 Liters
15.47 Liters
14.90 Liters Mass Uqujd
Charcoal tube sample Styrene concentration = Mass , iqujd =
Volume 5Undart
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
17:03
18:03
1.3%
2.20
0.1476
34.1
Milligrams
mg/liter
ppm
Pressure barometric
Vacuum „„.,„
Temperature^^
NDA-7-1 Initial Volume
Final Volume
Volume
1.017
28.92 inches of mercury
1.0 inches of mercury
88 ° Fahrenheit
1485.67 Liters
1500.69 Liters
15.02 Liters
14.07 Liters
Meter VOST3
Start Time 14:50
Finish Time 15:50
Moisture 1.1%
Mass
Charcoal tube sample Styrene concentration
Concentration, pan per million (ppm)
Mass
Volume
ug/liter x 24.04 liter/mole
molecular weight
Detection Limit
0.01 Milligrams
0.0007 mg/liter
0.2 ppm
Page 2
-------
Condition 7 Method 18 Sampling Results
Y =
Pressure bmaaac
Vacuum maa
Temperaturemaer
NDB-7-2 Initial Volume
Final Volume
Volume—™
1.017
28.92 inches of mercury
1.0 inches of mercury
90 ° Fahrenheit
1500.77 Liters
1515.80 Liters
15.03 Liters
Volume SUD(tanl 14.06 Liters
Charcoal tube sample Styrene concentration = Mass Liquid
Volume jundanj
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 3
Start Time 17:03
Finish Time 18:03
Moisture 0.9%
Detection Limit
Mass Liquid 0.01 Milligrams
0.0007 mg/liter
= 0.2 ppm
Page3
-------
Condition 8 Method 18 Sampling Results
Y = 0.997
Pressure baiomeaic 29.50 inches of mercury Meter
Vacuum meter 1.0 inches of mercury Start Time
Temperaturemettr 49 ° Fahrenheit Finish Time
ME-8-1 Initial Volume 2315.23 Liters Moisture
Final Volume 2318.43 Liters
Volumemner 3.20 Liters
Volume sun(tani 3.22 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume sundart
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weieht
VOST2
7:58
8:13
1.2%
2.17
0.6731
155.4
Milligrams
mg/liter
ppm
Y = 0.999
Pressure hironOTnc 29.50 inches of mercury Meter
Vacuum mner 1.0 inches of mercury Start Time
Temperaturemettr 49 ° Fahrenheit Finish Time
RE-8-1 Initial Volume 7741.94 Liters Moisture
Final Volume 7746.40 Liters
Volumemaer 4.46 Liters
Volume iaaauA 4.51 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass | iquid =
Volume 5an(tanl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST1
7:58
8:28
1.0%
0.74
0.1640
37.9
Milligrams
mg/liter
ppm
Pressure,
Vacuum ,«„»
Temperature.^
9-8-2
Initial Volume
Final Volume
Volume
1.052
29.50 inches of mercury
0.0 inches of mercury
83 ° Fahrenheit
56.36 Liters
71.53 Liters
15.17 Liters
15.04 Liters
Meter ES-1
Start Time 9:21
Finish Time 10:21
Moisture 1.7%
Mass
Charcoal tube sample Styrene concentration = Mass u
Concentration, pan per million (ppm)
Volume
ug/liter x 24.04 liter/mole
molecular weight
Detection Limit
0.01 Milligrams
0.0007 mg/liter
0.2 ppm
Pagel
-------
Condition 8 Method 18 Sampling Results
Y =
Pressure baranaric
Vacuum maa
Temperaturemettr
10-8-1 Initial Volume
Final Volume
Volumemaer
Volume i0aaui
1.052
29.50 inches of mercury Meter
0.0 inches of mercury Start Time
73 ° Fahrenheit Finish Time
43.55 Liters Moisture
56.23 Liters
12.68 Liters
12.86 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume sun(tan,
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
7:54
8:46
1.3%
0.40 Milligrams
0.0311 mg/liter
7.2 ppm
Y = 1.017
Pressure tare™™ 29.50 inches of mercury
Vacuum man. 1.0 inches of mercury
Temperature,,,,^ 78 ° Fahrenheit
NDA-8-1 Initial Volume
Final Volume
Volume,,^
Volume jumfcrf
1515.89 Liters
1529.05 Liters
13.16 Liters
12.82 Liters
Charcoal tube sample Styrene concentration = Mass Uquid
Concentration, pan per million
Volume sandlnl
(ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 3
Start Time 7:55
Finish Time 8:45
Moisture 1.0%
Detection Limit
Mass Uquid 0.01 Milligrams
0.0008 mg/liter
= 0.2 ppm
Pressure ^
Vacuum
Temperature,^
NDB-8-2 Initial Volume
Final Volume
Volume
1.017
29.50 inches of mercury
1.0 inches of mercury
84 ° Fahrenheit
1529.14 Liters
1543.75 Liters
14.61 Liters
14.08 Liters
Meter VOST 3
Start Time 9:21
Finish Time 10:21
Moisture 1.0%
Mass
Charcoal tube sample Styrene concentration =
Mass
Liquid
Volume
Concentration, pan per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
0.02 Milligrams
0.0014 mg/liter
0.3 ppm
Page 2
-------
Condition 9 Method 18 Sampling Results
Y =
Pressure barometric
Vacuum mnn
Temperaruremner
ME-9-1
Initial Volume
Final Volume
Volumemeter
0.997
29.28 inches of mercury
1.0 inches of mercury
71 ° Fahrenheit
2318.52 Liters
2321.43 Liters
2.91 Liters
Volume sundanl 2.78 Liters
Charcoal tube sample Styrene concentration =
Mass t iquid
Volume
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
_ molecular weight
Meter VOST 2
Start Time 18:03
Finish Time 18:18
Moisture 1.6%
MassUquid 1.91 Milligrams
0.6869 mg/liter
= 158.6 ppm
: Y =
Pressure baranelric
' Vacuum mner
Temperaturemaer
RE-9-1 Initial Volume
Final Volume
VolumemeUT
0.999
29.28 inches of mercury
1.0 inches of mercury
69 ° Fahrenheit
7746.60 Liters
7750.54 Liters
3.94 Liters
Volume itianui 3-81 Liters
Charcoal tube sample Styrene concentration =
Mass
Liqujd
Volume
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 1
Start Time 18:03
Finish Time 18:33
Moisture 0.8%
Mass Uquid 0.36 Milligrams
= 0.0944 mg/liter
21.8 ppm
Y =
Pressure ^mamc
Vacuum „„„
Temperaturemoef
9-9-1
Initial Volume
Final Volume
1.052
29.50 inches of mercury
0.0 inches of mercury
87 ° Fahrenheit
71.73 Liters
83.34 Liters
11.61 Liters
Meter ES-1
Start Time 18:04
Finish Time 18:50
Moisture 4.5%
Volume juafcrt 11.11 Liters
Charcoal tube sample Styrene concentration =
Mass
Mass
Volume jnaunj
Concentration, part per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
0.05 Milligrams
0.0045 mg/liter
= 1.0 ppm
Pagel
-------
Condition 9 Method 18 Sampling Results
Y = 1.017
Pressure ^ramam 29.28 inches of mercury
Vacuum maa 1.
TemperaruremMT 8
NDA-9-1 Initial Volume
Final Volume
Volumemaer
Volume suodlud
0 inches of mercury
8 ° Fahrenheit
1543.88 Liters
1550.65 Liters
6.77 Liters
6.44 Liters
Charcoal tube sample Styrene concentration = Mass Uqui(1
Concentration, pan per million
Volume sundlrd
(ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 3
Start Time 18:02
Finish Time 18:32
Moisture 0.8%
Detection Limit
Mass Liquid 0.01 Milligrams
0.0016 mg/liter
= 0.4 ppm
Page 2
-------
Condition 10 Method 18 Sampling Results
Y =
Pressure baromnric
Vacuum maa
Temperaturemner
ME-10-1 Initial Volume
Final Volume
Volumemner
0.999
29.28 inches of mercury
1.0 inches of mercury
70 ° Fahrenheit
2321.57 Liters
2323.45 Liters
1.88 Liters
Volume 5Un(linl 1.81 Liters
Charcoal tube sample Styrene concentration =
Mass
Liquid
Meter VOST 1
Stan Time 19:36
Finish Time 19:51
Moisture 1.4%
Mass Liquid XXXX Milligrams
= ######## mg/liter
Volume sun(Urd
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
ppm
RE-10-1
Y =
Pressure biromnric
Vacuum mn£r
Temperaniremncr
Initial Volume
Final Volume
Volumemner
Volume
sundlixl
0.999
29.28 inches of mercury
1.0 inches of mercury
71 ° Fahrenheit
7750.86 Liters
7755.23 Liters
4.37 Liters
4.22 Liters
Meter VOST 1
Start Time 19:36
Finish Time 20:06
Moisture 0.6%
Mass u
Charcoal tube sample Styrene concentration =
Mass
i.iquid
Volume sundinl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.10 Milligrams
= 0.0237 mg/liter
5.5 ppm
Pressure ,„„,„„„*
Vacuum „,«,
10-10-1
Initial Volume
Final Volume
Volume
1.052
29.50 inches of mercury
0.0 inches of mercury
85 ° Fahrenheit
83.47 Liters
98.21 Liters
14.74 Liters
14.78 Liters
Meter ES-1
Start Time 20:00
Finish Time 20:54
Moisture 0.2%
Mass
Charcoal tube sample Styrene concentration =
Mass
Volume
Concentration, part per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
3.11 Milligrams
0.2104 mg/liter
48.6 ppm
Page 1
-------
Condition 10 Method 18 Sampling Results
Y = 1.017
Pressure baroniaiic 29.28
Vacuum maa 1.0
Temperature,^, 89
NDA-10-1 Initial Volume
Final Volume
Volumemaer
Volume sund2ni
inches of mercury Meter
inches of mercury Start Time
0 Fahrenheit Finish Time
1550.75 Liters Moisture
1558.39 Liters ;
7.64 Liters
1
7.25 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass , iquid =
Volume SUIxUrt
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 3 ;
18:02
18:32
0.8%
:'.i
Detection Limit
0.01 Milligrams
0.0014 mg/liter
0.3 ppm
Page 2
-------
Condition 11 Method 18 Sampling Results
Y = 0.997
29.48 inches of mercury
1.0 inches of mercury
56 ° Fahrenheit
2323.57 Liters
2325.43 Liters
1.86 Liters
Pressure
Vacuum mua
Temperaturemarr
ME-11-1 Initial Volume
Final Volume
Volumemner
Volume sundln, 1.84 Liters
Charcoal tube sample Styrene concentration =
Mass
Liqilid
Volume,
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 2
Stan Time 9:13
Finish Time 9:28
Moisture 1.4%
Mass Liquid 0.99 Milligrams
0.5370 mg/liter
124.0 ppm
Pressure blroniaric
Vacuum mner
Temperature,,,™,
ME-11-2
Initial Volume
Final Volume
Volumemner
0.997
29.48 inches ot mercury
1.0 inches of mercury
75 ° Fahrenheit
2325.50 Liters
2328.03 Liters
2.53 Liters
Meter VOST 2
Start Time 10:39
Finish Time 10:59
Moisture 1.7%
Volume sun(tart 2.41 Liters
Charcoal rube sample Styrene concentration =
Mass Liquid
Mass u
Volume sun(tanl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
1.20 Milligrams
0.4977 mg/liter
114.9 ppm
Pressure
Vacuum ,„„,
Temperarurenau,
RE-11-1
Initial Volume
Final Volume
Volume
0.999
29.48 inches of mercury
1.0 inches of mercury
58 ° Fahrenheit
7756.17 Liters
7760.17 Liters
4.00 Liters
3.98 Liters
Meter VOST 1
Start Time 9:13
Finish Time 9:45
Moisture 0.9%
Mass
Charcoal tube sample Styrene concentration =
Volume
Concentration, pan per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
0.31 Milligrams
0.0779 mg/Hter
18.0 ppm
Pagel
-------
Condition 11 Method 18 Sampling Results
Pressure biromeuic
Vacuum maa
TemperaturemnCT
RE-11-3
Initial Volume
Final Volume
VolumemBCT
0.999
29.25 inches of mercury
1.0 inches of mercury
78 ° Fahrenheit
7762.90 Liters
7766.65 Liters
3.75 Liters
Volume sundird 3.57 Liters
Charcoal tube sample Styrene concentration =
Mass Uquid
Volume
Concentration, pan per million (ppm) = ug/h'ter x 24.04 liter/mole
molecular weight
Meter VOST 1
Start Time 12:01
Finish Time 12:31
Moisture 0.8%
Mass Liquid 0.13 Milligrams
0.0365 mg/liter
= 8.4 ppm
Y = 1.052
Pressure barometric 29.48
V" Vacuum mBer 0.0
a Temperaruremeur 86
9-11-2 Initial Volume
Final Volume
Volumemettr
Volume ,„„„,„,
inches of mercury
inches of mercury
0 Fahrenheit
113.83 Liters
125.18 Liters
11.35 Liters
11. 32 Liters
Charcoal rube sample Styrene concentration = Mass Uquid
Volume sundart
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter ES-1
Start Time 10:38
Finish Time 1 1 :20
Moisture 0.5%
Detection Limit
Mass Li^ 0.01 Milligrams
0.0009 mg/liter
= 0.2 ppm
Y = 1.052
Pressure taromaric 29.48
Vacuum „,«, 0.0
Temperature,^ 83
10-11-1 Initial Volume
Final Volume
Volume^ne,
Volume jnnfcrt
inches of mercury Meter
inches of mercury Start Time
"Fahrenheit Finish Time
98.30 Liters Moisture
113.78 Liters
15.48 Liters
15.60 Liters Mass u^
Charcoal tube sample Styrene concentration = Mass uquid -
Volume matud
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
9:12
10:12
0.0%
1.28 Milligrams
0.0821 mg/liter
18.9 ppm
Page 2
-------
Condition 11 Method 18 Sampling Results
Pressure barometric
Vacuum maa
TemperaturemnCT
NDA-11-1 Initial Volume
Final Volume
VolumemMr
1.017
29.48 inches of mercury
1.0 inches of mercury
82 ° Fahrenheit
1558.44 Liters
1572.84 Liters
14.40 Liters
Volume sunitani 13.94 Liters
Charcoal tube sample Styrene concentration = Mass Uquid
Volume
standard
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 3
Stan Time 9:14
Finish Time 10:14
Moisture 0.8%
Detection Limit
Mass Liqui<, 0.01 Milligrams
= 0.0007 mg/liter
= 0.2 ppm
PageS
-------
Condition 12 Method 18 Sampling Results
Y =
Pressure barometric
Vacuum mner
Temperaturemner
ME-12-1 Initial Volume
Final Volume
VolumemBcr
0.997
29.30 inches of mercury
1.0 inches of mercury
59 ° Fahrenheit
2331.30 Liters
2333.12 Liters
1.82 Liters
Volume sundar(l 1.78 Liters
Charcoal tube sample Styrene concentration =
Mass
Liquid
Volume suuxtart
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 2
Start Time 8:37
Finish Time 8:52
Moisture 1.7%
Mass Liquid 0.67 Milligrams
0.3770 mg/liter
87.0 ppm
Y = 0.997
Pressure barometric 29.30 inches of mercury Meter
Vacuum maa 1 .0 inches ot mercury Start Time
Temperaturemner 69 ° Fahrenheit Finish Time
ME-12-3 Initial Volume 2335.59 Liters Moisture
Final Volume 2344.22 Liters
Volumemner 8.63 Liters
Volume sandlnl 8.28 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume sandlnl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 2
11:05
12:05
1.6%
2.96 Milligrams
0.3577 mg/liter
82.6 ppm
Pressure
Vacuum
AF-12-1 Initial Volume
Final Volume
Volume,^,
0.999
29.30 inches of mercury
1.0 inches of mercury
59 ° Fahrenheit
7767.00 Liters
7770.90 Liters
3.90 Liters
Meter VOST 1
Start Time 8:37
Finish Time 9:07
Moisture 1.7%
Volume jnntont 3.82 Liters
Charcoal tube sample Styrene concentration =
Mass
Mass
Liquid
Volume
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.81 Milligrams
0.2123 mg/liter
= 49.0 ppm
Pagel
-------
Condition 12 Method 18 Sampling Results
Y = 0.997
Pressure hJroBieiric 29.30 inches of mercury Meter
Vacuum mOCT 1 .0 inches of mercury Start Time
TemperaturemnCT 74 ° Fahrenheit Finish Time
AF-12-4 Initial Volume 2344.42
Final Volume 2354.13
Volume,,^ 9.71
Volume sundiinl 9.22
Charcoal tube sample Styrene concentration
Concentration, part per million (ppm) =
Liters Moisture
Liters
Liters
Liters Mass Liquid
Mass Liquid
Volume sundiuxl
ug/liter x 24.04 liter/mole =
molecular weight
VOST2
12:31
13:31
1.6%
1.6 Milligrams
0.1735 mg/liter
40.0 ppm
Y = 1.052
Pressure bjrom£tric 29.30 inches of mercury Meter
Vacuum maer 0.0 inches of mercury Start Time
Temperaturemeler 84 ° Fahrenheit Finish Time
9-12-3 Initial Volume 1142.01 Liters Moisture
Final Volume 1155.51 Liters
Volume,^ 13.50 Liters
Volume sundlrt 13.09 Liters Mass Liqui(,
Charcoal tube sample Styrene concentration = Mass Liqui
-------
Condition 12 Method 18 Sampling Results
Y =
Pressure baromaric
Vacuum mtta
Temperature,^,
0-12-4
Initial Volume
Final Volume
Volumemaer
Volume
standard
1.052
29.30 inches of mercury
0.0 inches of mercury
84 ° Fahrenheit
1155.52 Liters
1169.89 Liters
14.37 Liters
13.98 Liters
Meter ES-1
Start Time 12:31
Finish Time 13:31
Moisture 2.7%
MaSS
!harcoal tube sample Styrene concentration = Mass Uquid
Volume ,un
-------
Condition 13 Method 18 Sampling Results
Y = 0.999
Pressure baromeuic 29.20 inches of mercury Meter
Vacuum mner 1 .0 inches of mercury Start Time
Temperaturemeur 72 ° Fahrenheit Finish Time
ME-13-2 Initial Volume 7800.15 Liters Moisture
Final Volume 7809.24 Liters
Volumema£r 9.09 Liters
Volume sunilinl 8.65 Liters Mass Uquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume sttn(Unj
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
VOST1
16:37
17:37
1.7%
1.78 Milligrams
0.2059 mg/liter
47.5 ppm
Y = 0.999
Pressure tamaunc 29.20 inches of mercury Meter
Vacuum maet 1.0 inches of mercury Stan Time
Temperature,,,,^ 67 ° Fahrenheit Finish Time
RE-13-1 Initial Volume 7792.50 Liters Moisture
Final Volume 7799.80 Liters
Volumemacr 7.30 Liters
Volume sundard 7.00 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Uqui
-------
Condition 13 Method 18 Sampling Results
Y =
Pressure baromeuic
Vacuum met£r
Temperaturemner
9-13-2
Initial Volume
Final Volume
VolumemnCT
Volume
1.052
29.20 inches of mercury
0.0 inches of mercury
86 ° Fahrenheit
1184.08 Liters
1199.07 Liters
14.99 Liters
14.64 Liters
Meter
Stan Time
Finish Time
ES-1
16:37
17:37
Moisture 1.6%
Mass
Liquid
Charcoal tube sample Styrene concentration = Mass, iquid
Volume sundart
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.09 Milligrams
0.0061 mg/liter'-
1.4 ppm
Y = 1.052
Pressure h;iroinmi<; 29.20 inches of mercury Meter
Vacuum maa 0.0 inches of mercury Start Time
Temperaturemaer 83 ° Fahrenheit Finish Time
HM3-1 Initial Volume 1170.11 Liters Moisture
Final Volume 1184.95 Liters
Volumemeler 14.84 Liters
Volume sandini 14.49 Liters Mass Uquid
Charcoal tube sample Styrene concentration = Mass ( iquid =
Volume !Undart
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
15:20
16:15
2.2%
5.35 Milligrams
0.3692 mg/liter
85.2 ppm
Y = 1.017
Pressure barometric 29.20 inches of mercury Meter
Vacuum „„„ 1 .0 inches of mercury Start Time
Temperature™^ 90 ° Fahrenheit Finish Time
NDA-13-1 Initial Volume 1602.48 Liters Moisture
Final Volume 1615.74 Liters
Volume™,,, 13.26 Liters
Volume joBtari 12.43 Liters Mass LU^
Charcoal tube sample Styrene concentration = Mass uquid -
Volume nuatarf
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST3
18:20
19:16
1.6%
0.09 Milligrams
0.0072 mg/liter
1.7 ppm
Page 2
-------
Condition 4 Method 18 Cumene Sampling-Results
Y =
Pressure ,,aroilianc
Vacuum mmr
TemperaturemetCT
NDA-4-1 Initial Volume
Final Volume
Volumemeter
1.017
28.80 inches of mercury
1.0 inches of mercury
90 ° Fahrenheit
1399.28 Liters
1413.68 Liters
14.40 Liters
Volume standanl 13.40 Liters
Charcoal tube sample Cumene concentration =
MaSS Liui
Volume
standard
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 3
Start Time 20:05
Finish Time 21:05
Moisture 1.0%
Mass uquid 0-14 Milligrams
0.0104 mg/liter
= 2.1 ppm
Pagel
-------
Condition 8 Method 18 Cumene Sampling Results
Y = 1.017
Pressure haronieuic 29.50
Vacuum maa 1.0
TemperaturemMt 78
NDA-8-1 Initial Volume
Final Volume
Volume™*,
Volume sundlrt
inches of mercury
inches of mercury
0 Fahrenheit
1515.89 Liters
1529.05 Liters
13.16 Liters
12.82 Liters
Charcoal tube sample Cumene concentration = Mass , ,iquid
Volume sull(tart
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Meter VOST 3
Start Time 7:55
Finish Time 8:45
Moisture 1.0%
Detection Limit
Mass Liquid 0-14 Milligrams
0.0109 mg/liter
= 2.2 ppm
Pagel
-------
Condition 10 Method 18 Cumene Sampling Results
Pressure,
Vacuum maa
TemperaturemBCT
RE-10-1 Initial Volume
Final Volume
Volumemaer
0.999
29.28 inches of mercury
1.0 inches of mercury
71 ° Fahrenheit
7750.86 Liters
7755.23 Liters
4.37 Liters
Volume 5laabrt 4.22 Liters
Charcoal tube sample Cumene concentration =
Mass
Liquid
Meter VOST 1
Start Time 19:36
Finish Time 20:06
Moisture 0.6%
Mass
Volume sundanj
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.13 Milligrams
0.0308 mg/liter
6.2 ppm
Pagel
-------
Method 18 Styrene Spiked Sampling Results
Y = 0.999
Pressure baromaric 29. 10 inches of mercury Meter
Vacuum mner 1.0 inches of mercury Start Time
Temperature.,^ 56 ° Fahrenheit Finish Time
MES-3-3 Initial Volume 7707.97 Liters Moisture
Final Volume 7710.02 Liters :
Volumemner 2.05 Liters
Volume sundanl 2.02 Liters Mass Uqui(1
Charcoal tube sample Styrene concentration = Mass Uquid =
Volume sundard
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 1
17:36
17:51
1.1%
3.24 Milligrams
1.6074 mg/litef
371.0 ppm
Y =
Pressure biromaric
Vacuum marr
Temperaturemettr
RES-4-1 Initial Volume
Final Volume
Volumemoer
Volume sundlrt
0.999
29.20 inches of mercury Meter
1 .0 incnes of mercury Stan Time
51 ° Fahrenheit Finish Time
7710.16 Liters Moisture
7712.11 Liters
1.95 Liters
1.95 Liters Mass Liqilid
Charcoal tube sample Styrene concentration = Mass Liquj<, =
Volume sundinl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 1 <
20:06
20:21
0.9%
0.52 Milligrams
0.2670 mg/liter
61.6 ppm
Y = 0.997
Pressure baroocnic 28.80 inches of mercury Meter
Vacuum „„.„, 1 .0 inches of mercury Stan Time
Temperature.,,^ 98 ° Fahrenheit Finish Time
AFS-5-2 Initial Volume 2300.34 Liters Moisture
Final Volume 2308.23 Liters
VolumCnae, 7.89 Liters
Volume janfcn, 7.01 Liters Mass u^
Charcoal tube sample Styrene concentration = Mass u^uid -
Volume jundanj
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 2
11:08
12:08
2.1%
1.86 Milligrams
0.2652 mg/liter
61.2 ppm
Pagel
-------
Method 18 Styrene Spiked Sampling Results
Y = 0.999
Pressure btmaaiK 28.78 inches of mercury Meter
Vacuum ,„„, 1 .0 inches of mercury Start Time
TemperaruremaCT 82 ° Fahrenheit Finish Time
MES-6-2 Initial Volume 7735.86 Liters Moisture
Final Volume 7737.38 Liters
VolumemaCT 1.52 Liters
Volume sttndu<1 1.39 Liters Mass Uquid
Charcoal tube sample Styrene concentration = Mass Liquid =
Volume Mauri
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST1
17:33
17:43
2.3%
2.48 Milligrams
1.7840 mg/liter
411.8 ppm
Y =
Pressure baraiieilic
Vacuum motr
Temperature^^,
MES-11-2 Initial Volume
Final Volume
Volumemaer
0.999
29.48 inches of mercury
1.0 inches of mercury
71 ° Fahrenheit
7760.25 Liters
7762.87 Liters
2.62 Liters
Volume san
-------
Method 18 Styrene Spiked Sampling Results
Y =
Pressure barommic
Vacuum mna
Temperaturemettr
MES-12-3 Initial Volume
Final Volume
Volumemettr
Volume sundarf
0.999
29.30 inches of mercury Meter
1 .0 inches of mercury Start Time
65 ° Fahrenheit Finish Time
7773.84 Liters Moisture
7782.78 Liters
8.94 Liters
8.66 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass , iqujd =
Volume suntanl
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST1
11:05
12:05
1.6%
4.90 Milligrams
0.5661 mg/liter
130.7 ppm
Y = 0.999
Pressure hJromanc 29.30 inches of mercury Meter
Vacuum maa 1.0 inches of mercury Start Time
Temperaturemettrv 68 ° Fahrenheit Finish Time
AFS-12-4 Initial Volume
Final Volume
Volumemeter
Volume suntanl
Charcoal tube sample Styrene
7783.41 Liters Moisture
7792.13 Liters
8.72 Liters
8.39 Liters Mass Liquid
concentration = Mass Liquid =
Volume juatani
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST 1
12:31
13:31
1.6%
1.87 Milligrams
0.2228 mg/liter
51.4 ppm
Page 3
-------
Condition 1 Method 18 Sampling Results - Methyl Methacrylate
Y = 0.997
Pressure banmCTic 28.92 inches of mercury Meter
Vacuum mna 0.0 inches of mercury Start Time
Temperaruremeler 71 "Fahrenheit Finish Time
ME-1-3 Initial volume 2268.33
Final Volume 2274.54
Volume^B, 6.21
Volume 5U1Mtard 5.71
Liters Moisture
Liters
Liters
Liters Mass LiqUi
-------
Condition 2 Method 18 Sampling Results - Methyl Methacrylate
Y = 0.997
Pressure birometrjc 28.84 inches of mercury Meter
Vacuum meler 1.0 inches of mercury Start Time
Temperaturemeter 69 ° Fahrenheit Finish Time
ME-2-1 Initial Volume 2275.08
Final Volume 2283.95
Volumemettr 8.87
Volume SBndird 8.38
Liters Moisture
Liters
Liters
Liters Mass Uquid
Charcoal tube Methyl Methacrylate concentration = Mass Liquid
Concentration, part per million (ppm) =
Volume standard
ug/liter x 24.04 liter/mole =
molecular weight
VOST2
20:23
20:54
1.5%
6.84 Milligrams
0.8162 mg/liter
227.9 ppm
Y = 0.999
Pressure hiromeujc 28.84 inches ot mercury Meter
Vacuum mtltt 1 .0 inches ot" mercury ; Start Time
Temperaturemeler 71 ° Fahrenheit , Finish Time
RE-2-1 Initial Volume 7679.50
Final Volume 7694.21
Volumemettr 14.71
Volume Slin
-------
Condition 1 Method 18 Sampling Results
Y =
Pressure biroreiric
Vacuum TOtw
Temperature™,,,
NDA-2-2 Initial Volume
Final Volume
Volumemw
Volume
itandird
1.017
28.84 inches of mercury
1.0 inches of mercury
87 ° Fahrenheit
1337.15 Liters
1351.81 Liters
14.66 Liters
13.73 Liters
Meter VOST 3
Start Time 22:00
Finish Time 23:00
Moisture 1.0%
Charcoal tube Methyl Methacrylate concentration = Mass Liquid
Volume ,undml
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
Mass Liqui(l 0.04 Milligrams
= 0.0029 mg/liter
= 0.8 ppm
Y =
Pressure ^aomeuK
Vacuum meta
TemperatureTCter
10-2-2 Initial Volume
Final Volume
Volumemeler
Volume sundlrt
1.052
28.80 inches of mercury
0.0 inches of mercury
87 ° Fahrenheit
881.65 Liters
897.00 Liters
15.35 Liters
14.78 Liters
Charcoal tube Methyl Methacrylate concentration = Mass Liquid
Volume ,landird
Concentration, part per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
Meter ES-1
Start Time 22:00
Finish Time 23:00
Moisture 1.5%
Detection Limit
Mass Ljqui<1 0.22 Milligrams
0.0149 mg/liter
= 4.2 ppm
Page 2
-------
Condition 2 Method 18 Sampling Results - Methyl Methacrylate
Y = 0.997
Pressure bin)llieiri(. 28.84 inches of mercury Meter
Vacuum meler 1 .0 inches of mercury Start Time
Temperaturemelw 69 ° Fahrenheit Finish Time
ME-2-1 Initial Volume 2275.08
Final Volume 2283.95
Volumemettr 8.87
Volume iaaaut 8.38
Liters Moisture
Liters
Liters
Liters Mass Liquid
Charcoal tube Methyl Methacrylate concentration = Mass Liquid =
Concentration, pan per million (ppm) =
Volume !iandard
ug/liter x 24.04 liter/mole =
molecular weight
VOST2
20:23
20:54
1.5%
6.84 Milligrams
0.8162 mg/liter
227.9 ppm
Y =
Pressure birOTOIric
Vacuum meler
Temperaturemettr
RE-2-1
Initial Volume
Final Volume
Volume-™
Volume
itindard
0.999
28.84 inches of mercury
1.0 inches of mercury
71 "Fahrenheit
7679.50 Liters
7694.21 Liters
14.71 Liters
13.93 Liters
Meter VOST 1
Start Time 20:20
Finish Time 21:22
Moisture 1.1%
Mass Liqi,uj 2.19 Milligrams
Charcoal tube Methyl Methacrylate concentration = Mass |.iqui
-------
Condition 2 Method 18 Sampling Results - Methyl Methacrylate
Y = 1.017
Pressure bmmar* 28.84
Vacuum meter 1 .0
Temperaturemeter 87
NDA-2-2 Initial Volume
Final Volume
Volumemett,
Volume ,„„„„„
inches of mercury Meter
inches of mercury Start Time
0 Fahrenheit Finish Time
1337.15 Liters Moisture
1351.81 Liters
14.66 Liters
13.73 Liters Mass Liqiji(i
Charcoal tube Methyl Methacrylate concentration = Mass Uquid =
Volume sundud
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST3
22:00
23:00
1.0%
0.04 Milligrams
0.0029 mg/liter
0.8 ppm
Y = 1.052
Pressure barometne 28.80
Vacuum meter 0.0
TemperatureTOttr 87
10-2-2 Initial Volume
Final Volume
Volumeraeler
Volume 5ttndird
inches of mercury ,; Meter
inches of mercury i. Start Time
0 Fahrenheit Finish Time
881.65 Liters Moisture
897.00 Liters
15.35 Liters
14.78 Liters Mass Liquid
Charcoal tube Methyl Methacrylate concentration = Mass Liquid =
Concentration, part per million
Volume jaildlrt
(ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-l
22:00
23:00
1.5%
Detection Limit
0.22 Milligrams
0.0149 mg/liter
4.2 ppm
Page 2
-------
Condition 3 Method 18 Sampling Results - Methyl Methacrylate
Y = 0.997
Pressure barometrjc 28.90
Vacuum meter 1.0
Temperaturemeter 64
ME-3-1 Initial Volume
Final Volume
Volumem(:ttr
Volume sundsrd
inches of mercury Meter
inches of mercury Start Time
0 Fahrenheit Finish Time
2287.47 Liters Moisture
2290.49 Liters
3.02 Liters
2.90 Liters Mass Uquid
Charcoal tube Methyl Methacrylate concentration = Mass Uquid =
Concentration, part per million
Volume SUJldard
(ppm) = ug/liter x 24.04 liter/mole i =
molecular weieht
VOST2
14:25
14:55
1.0%
0.07 Milligrams
0.0241 mg/liter
6.7 ppm
Y = 0.997
Pressure b>romwie 29.10 inches ot mercury ' Meter
Vacuum maa 1 .0 inches of mercury • v: Start Time
Temperaturemeter 57 ° Fahrenheit Finish Time
ME-3-3 Initial Volume 2293.37
Final Volume 2294.61
VolumeTCBt 1.24
Volume sundlrt 1.21
Liters Moisture
Liters
Liters
Liters Mass Liquid
Charcoal tube Methyl Methacrylate concentration = Mass ( iquld =
Concentration, pan per million (ppm) =
Volume ,UI)liU(1
ug/liter x 24.04 liter/mole =
molecular weight
VOST2
17:35
17:50
1.1%
0.04 Milligrams
0.0329 mg/liter
9.2 ppm
Pagel
-------
Condition 4 Method 18 Sampling Results - Methyl Methacrylate
Y = 1.052
Pressure biromemc 28.80 inches of mercury Meter
Vacuum TOIer 0.0 inches of mercury Start Time
Temperaturemettr 90 ° Fahrenheit Finish Time
9-4-2 Initial Volume 941.12
Final Volume 956.55
VolumemM, 15.43
Volume sundlrt 14.82
Liters Moisture
Liters
Liters
Liters Mass Liqu,d
Charcoal tube Methyl Methacrylate concentration = Mass Liqui(l =
Concentration, part per million (ppm) =
Volume jamjjrt
ug/liter x 24.04 liter/mole =
molecular weight
ES-1
21:40
22:30
1.2%
0.08 Milligrams
0.0054 mg/liter
1.5 ppm
Pagel
-------
Condition 5 Method 18 Sampling Results - Methyl Methacrylate
Y =
Pressure ban>melric
Vacuum mwr
Temperaturemtler
RE-5-1
Initial Volume
Final Volume
Volumemeler
0.999
28.85 inches of mercury
1.0 inches of mercury
79 ° Fahrenheit
7713.90 Liters
7720.65 Liters
6.75 Liters
Volume sun(tafd 6.24 Liters
Charcoal tube Methyl Methacrylate concentration = Mass Liauid
Meter VOST 1
Stan Time 9:04
Finish Time 9:49
Moisture 2.1%
Mass Liquui 0.05 Milligrams
= 0.0080 mg/liter
Volume j
Concentration, part per million (ppm) = ug/liter x 24,04 liter/mole
molecular weight
2.2 ppm
.;>• Y =
pressure biromelrie
Vacuum meler
Temperaturemeler
10-5-2 Initial Volume
Final Volume
Volumem,»,
Volume
itandird
1.052
29.25 inches of mercury
0.0 inches of mercury
91 ° Fahrenheit
972.65 Liters
987.82 Liters
15.17 Liters
14.58 Liters
Charcoal tube Methyl Methacrylate concentration = Mass Liquid
Volume
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
_ _ • _ _ molecular weight _
Meter ES-1
Stan Time 11:08
Finish Time 12:08
Moisture 2.5%
Mass Liquid 0.05 Milligrams
= 0.0034 mg/liter
= 1.0 ppm
Pagel
-------
Condition 6 Method 18 Sampling Results - Methyl Methacrylate
Pressure baromeiric
Vacuum mm
TemperatureTOttr
ME-6-2 Initial Volume
Final Volume
VolumeraMr
Volume J
0.997
28.78 inches of mercury
1.0 inches of mercury
78 ° Fahrenheit
2308.46 Liters
2310.28 Liters
1.82 Liters
1.67 Liters
Meter VOST2
Start Time 17:33
Finish Time 17:43
Moisture 2.3%
; Mass Liquid
Charcoal tube Methyl Methacrylate concentration = Mass
Volume 5Undlfd
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.10 Milligrams
0.0598 mg/liter
16.7 ppm
Y =
Pressure tmomm
Vacuum ^^
10-6-1
Initial Volume
Final Volume
Volume™
1.052
29.20 inches of mercury
0.0 inches of mercury
93 ° Fahrenheit
987.85 Liters
1001.42 Liters
13.57 Liters
Volume Jttnitanl 13.00 Liters
Charcoal tube Methyl Methacrylate concentration = Mass Liquid
Volume j
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
_ molecular weight
Meter ES-1
Start Time 16:05
Finish Time 16:58
Moisture 2.3%
Mass Liquid 0-05 Milligrams
0.0038 mg/liter
= 1.1 ppm
Pagel
-------
Condition 7 Method 18 Sampling Results - Methyl Methacrylate
Y =
Pressure biromeme
Vacuum meler
Temperaturemeter
ME-7-1 Initial Volume
Final Volume
Volumemeler
Volume jan(tari
0.997
28.92 inches of mercury Meter
1 .0 inches of mercury Start Time
77 ° Fahrenheit Finish Time
2310.34 Liters Moisture
2312.66 Liters
2.32 Liters
2. 16 Liters Mass Uqui(1
Charcoal tube Methyl Methacrylate concentration = Mass Uquid =
Volume !laiutar(1
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST2
14:49
15:04
1.8%
0.29 Milligrams
0. 1343 mg/liter
31.0 ppm
Y =
'.Pressure blfonione
Vacuum meler
Temperaturemeler
ME-7-3 Initial Volume
Final Volume
Volumemett,
Volume ianlui
0.997
28.92 inches of mercury Meter
1 .0 inches of mercury Start Time
66 ° Fahrenheit Finish Time
2312.80 Liters Moisture
2315.10 Liters
2.30 Liters
2.19 Liters Mass LiqUu,
Charcoal tube Methyl Methacrylate concentration = Mass UqM =
Volume ,undir(1
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST2
19:13
19:28
1.4%
0.36 Milligrams
0.1641 mg/liter
45.8 ppm
Y = 1.052
Pressure ^ma,* 28.92 inches of mercury Meter
Vacuum mat, 0.0 inches of mercury Start Time
Temperaturemeter 90 ° Fahrenheit Finish Time
10-7-2 Initial Volume 28. 15 Liters . Moisture
Final Volume 43.62 Liters
Volume^ 15.47 !,..icrs
Volume ilanltanl 14.90 Liters Mass Liquid
Charcoal tube Methyl Methacrylate concentration = Mass Uquid =
Volume jantml
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
ES-1
17:03
18:03
1.3%
0. 17 Milligrams
0.0114 mg/liter
3.2 ppm
Pagel
-------
Condition 9 Method 18 Sampling Results - Methyl Methacrylate
Y = 0.999
Pressure ^moric 29.28 inches of mercury Meter
Vacuum mem I .0 inches of mercury Start Time
Temperatureraeler 69 ° Fahrenheit Finish Time
RE-9-1 Initial Volume 7746.60
Final Volume 7750.54
Volumeraettr 3.94
Volume ,„„,„„ 3.81
Liters Moisture
Liters
Liters
Liters Mass Uquj(1
Charcoal tube Methyl Methacrylate concentration = Mass uquuj =
Concentration, part per million (ppm) =
Volume jandlnl
ug/liter x 24.04 liter/mole =
molecular weight
VOST 1
18:03
18:33 :
0.8%
0.04 Milligrams
0.0105 mg/liier
2.9 ppm
Pagel
-------
Condition 12 Method 18 Sampling Results - Methyl Methacrylate
Y =
Pressure baromMic
Vacuum meter
Temperaruremeler
9-12-3
1.052
29.30 inches of mercury
0.0 inches of mercury
84 ° Fahrenheit
1142.01 Liters
1155.51 Liters
13.50 Liters
13.09 Liters
Charcoal rube Methyl Methacrylate concentration = Mass uquid
Volume MIxUrd
Initial Volume
Final Volume
Volumemeler
Volume
Meter ES-1
Start Time 11:05
Finish Time 12:04
Moisture 3.0%
Mass Liquid 0.04 Milligrams
0.0031 mg/liter
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
0.9 ppm
Pagel
-------
Condition 13 Method 18 Sampling Results - Methyl Methacrylate
Y =
Pressure bjromeffic
Vacuum mettr
Temperaturemeler
9-13-2
Initial Volume
Final Volume
Volumemeter
1.052
29.20 inches of mercury
0.0 inches of mercury
86 ° Fahrenheit
1184.08 Liters
1199.07 Liters
14.99 Liters
Volume sandinl 14.64 Liters
Charcoal tube Methyl Methacrylate concentration =
Mass Uquid
Volume S
Concentration, pan per million (ppm)
ug/liter x 24.04 liter/mole
molecular weicht
Meter ES-1
Start Time 16:37
Finish Time 17:37
Moisture 1.6%
Mass luid 0.25 Milligrams
= 0.0171 mg/liter
= 4.8 ppm
Pagel
-------
Method 18 Sampling Results of Styrene Cylinders
Y = 1.017
Pressure baroineuic 29.20
Vacuum maa 1.5
Temperature,^,. 88
250.7 ppm Initial Volume
Final Volume
VolumemMt
Volume sundlrt
inches of mercury Meter
inches of mercury Stan Time
"Fahrenheit Finish Time
20. 10 Liters Moisture
26. 10 Liters
6.00 Liters
5.74 Liters Mass Liquid
Charcoal tube sample Styrene concentration = Mass Liquid * =
Concentration, pan per million
Volume standard
(ppm) = ug/liter x 24.04 liter/mole =
molecular weight
VOST3
17:12
17:19
0.0%
2.62
0.4562
105.3
<"
Milligrams
mg/liter
ppm
Y =
Pressure hiromethc
Vacuum maa
Temperaturemettr
143.1 ppm initial Volume
Final Volume
Volumemeu,
1.017
29.20 inches of mercury
1.5 inches of mercury
88 ° Fahrenheit
30.91 Liters
36.91 Liters
6.00 Liters
Meter VOST 3
Start Time 17:33
Finish Time 17:39
Moisture 0.0%
Volume sundlri 5.74 Liters
Charcoal tube sample Styrene concentration =
Mass
Liquid
Mass LI
Volume
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole
molecular weight
1.84 Milligrams
0.3207 mg/liter
74.0 ppm
1.017
29.20 inches of mercury
1.5 inches of mercury
89' Fahrenheit
50.00 Liters
56.00 Liters
6.00 Liters
Volume juafcrf 5.73 Liters
Charcoal tube sample Styrene concentration =
Pressure
Vacuum
Temperaturenne,
102 ppm Initial Volume
Final Volume
Meter VOST 3
Start Time 18:10
Finish Time 18:16
Moisture 0.0%
Mass
Mass
Volume
Concentration, part per million (ppm)
ug/liter x 24.04 liter/mole
molecular weight
1.76 Milligrams
0.3073 mg/liter
= 70.9 ppm
Pagel
-------
LASCO
Styrene Bag Standards
Response Factors
BAG
Run 1
Run 2
Run 3
Run 4
Run 5
Run 6
Run?
Run 8
Styrene Injection
ppm Styrene
67.7
67.9
134.6
189.8
362.2
557.3
1106.2
1659.5
JUM 1 Response
ppm Propane
161.1
160.3
319.0
441.3
855.9
1266
2636
3983
Response
Factor
0.4202
0.4236
0.4219
0.4301
0.4232
0.4402
0.4197
0.4166
Average 0.4244
Average 0.4263
Standard Deviation 0.75%
JUM 5 Response
ppm Propane
156.9
157.8
316.3
431.4
843.9
1250
2642
4103
Response
Factor
0.4315
0.4303
0.4255
0.4400
0.4292
0.4458
0.4187
0.4045
Average 0.4282
Standard Deviation 1 .27 %
Styrene Cylinders
102
143.1
250.7
JUM 1 Response
ppm Propane
253.3
293.2
411.0
Response
Factor
0.4027
0.4881
0.6100
JUM 5 Response
ppm Propane
250.0
290.3
409.1
Response
Factor
0.4080
0.4929
0.6128
Pagel
-------
• -'^if
PACIFIC ENVIRONMENTAL SERVICES, INC.
Project No.
S40S.OD3
Page
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Prepared By Date Checked By Date Sheet Title
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PACIFIC ENVIRONMENTAL SERVICES, INC.
Project No.
S405.003
Page
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Client
Location
Prepared By Date Checked By Date Sheet Title
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WASHINGTON, DC • RESEARCH TRIANGLE PARK, NC • LOS ANGELES. CA« CINCINNATI. OH
-------
Styrene Bag Standards
Y = 0.980
Pressure baromaiic 29.05
inches of mercury
Pressure mner 12.6 inches of water
Temperaturemner 81
BAG 1 Initial volume
Final Volume
Volumemner
Volume saaaatA
Bag sample VOC concentration
Concentration, pan per million
0 Fahrenheit
3674.32 Liters INJECTION 1 Initial mass
3754.32 Liters Final mass
80.00 Liters Total mass
76.66 Liters • Mass Uquid
(mg/Liter) = Mass Liqui(1 =
Volume S12nitar(j
(ppm) = ug/liter x 24.04 liter/mole =
molecular weight
16.6085 Grams
16.586 Grams
0.0225 Grams
22.5 Milligrams
0.2935 mg/liter
67.7 ppm
Y =
Pressure haroraelnc
Pressure mnn
Temperaturemnn
BAG 2 Initial volume
Final Volume
Volumemner
Volume jundjni
0.980
28.99 inchesVb'f mercury
12.6 inches of water
81 ° Fahrenheit
3892.85 Liters INJECTION 2 Initial mass
3972.85 Liters Final mass
80.00 Liters Total mass
76.51 Liters ' Mass Liquid
Bag sample VOC concentration (mg/Liter) = Mass Liquid =
Volume notort
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
16.6053 Grams
16.5828 Grams
0.0225 Grams
22.5 Milligrams
0.2941 mg/liter
67.9 ppm
Y = 0.980
Pressure baromaiic 28.99 inches of mercury
Pressure „„,„ 12.6 inches of water
Temperature,^ 81 ° Fahrenheit
BAG 3
Initial volume
Final Volume
Volumemaer
Volume jnntart
Bag sample VOC concentration
Concentration, part per million
3982.35 Liters
4062.35 Liters
80.00 Liters
76.51 Liters
(mg/Liter) =
(ppm) = ug/liter
INJECTION 3A Initial mass
Final mass
INJECTION 3B Initial mass
Final mass
Total mass
MaSS Li,,^
MaSS uqui, . .=
Volume joatart
x 24.04 liter/mole =
16.6048 Grams
16.5825 Grams
16.6046 Grams
16.5823 Grams
0.0446 Grams
44.6 Milligrams
0.5830 mg/liter
134.6 ppm
molecular weight
-------
Styrene Bag Standards
Y = 0.980
Pressure hjromeuic 28.99 inches of mercury
Pressure mner 12.6 inches of water
Temperaturemncr 86 ° Fahrenheit
BAG 4 Initial volume 4172.85 Liters INJECTION 4 Initial mass
Final Volume 4264.85 Liters Final mass
Volumemnrr 92.00 Liters Total mass
Volume suntod 87.18 Liters Massed
Bag sample VOC concentration (mg/Liter) = Mass Uqu^ =
Volume ,,Jnrt.M
Concentration, pan per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
15.0931 Grams
15.0214 Grams
0.0717 Grams
71.7 Milligrams
0.8225 mg/liter
189.8 ppm
Y = 0.980
Pressure ^nmain 28.99 inches of mercury
Pressure maa 12.6 inches of water
TemperaturCmae, 89.5 ° Fahrenheit
BAG 5 Initial volume 4268.73 Liters INJECTION 5 Initial mass
Final Volume 4353.73 Liters Final mass
Volumcmaj, 85.00 Liters Total mass
Volume saalut 80.03 Liters Mass Uquid
Bag sample VOC concentration (mg/Liter) = Mass Uquid =
Volume jo,,,,,,,,
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
15.1478 Grams
15.0222 Grams
0. 1256 Grams
125.6 Milligrams
1.5694 mg/liter
362.2 ppm
Y = 0.980
Pressure barometric 28.99 inches of mercury
Pressure „„„ 12.6 inches of water
Temperaturemae, 91.5 ° Fahrenheit
BAG 6 Initial volume 4366.7 Liters INJECTION 6 Initial mass
Final Volume 4446.7 Liters Final mass
Volume^,, 80.00 Liters Total mass
Volume ...^.^ 75.05 Liters Mass u^
Bag sample VOC concentration (mg/Liter) = Mass uquid =*
Volume njahn,
Concentration, part per million (ppm) = ug/liter x 24.04 liter/mole =
molecular weight
15.2034 Grams
15.0222 Grams
0.1812 Grams
181.2 Milligrams
2.4144 mg/liter
557.3 ppm
-------
Styrene Bag Standards
Y = 0.980
Pressure barometric 28.99 inches of mercury
Pressure melcr 12.6 inches of water
Temperaturemeter 91 ° Fahrenheit
BAG 7 Initial volume
Bag
Final Volume
VolumemeICT
Volume sundart
sample VOC concentration
Concentration, pan per million
4456.2 Liters
4536.2 Liters
80.00 Liters
75.12 Liters
(mg/Liter) =
(ppm) = ug/liter
INJECTION 7A Initial mass
Final mass
INJECTION 7B Initial mass
Final mass
Total mass
MaSS Liquid
MaSS Liquid =
Volume junoanj
x 24.04 liter/ mole =
15.2018 Grams
15.0222 Grams
15.2028 Grams
15.0224 Grams
0.3600 Grams
360 Milligrams
4.7924 mg/liter
1 106.2 ppm
molecular weight
Y = 0.980
Pressure barometric 28.99 inches of mercury
Pressure mafr 12.6 inches of water
Temperaturemeter 92 ° Fahrenheit
BAGS
Initial volume
Final Volume
Volumemner
Volume sundird
Bag sample VOC concentration
Concentration, pan per million
4550.4 Liters
4630.4 Liters
80.00 Liters
74.98 Liters
(mg/Liter) =
(ppm) = ug/liter
INJECTION 8A Initial mass
Final mass
INJECTION 8B Initial mass
Final mass
INJECTION 8C Initial mass
Final mass
Total mass
Mass Liquid
MaSS Liquid -
Volume jundinl
x 24.04 liter/mole =
15.2030 Grams
15.0228 Grams
15.2022 Grams
15.0224 Grams
15.2016 Grams
15.0225 Grams
0.5391 Grams
539.1 Milligrams
7.1897 mg/liter
1659.5 ppm
molecular weight
-------
LASCO
Styrene Bag Standards
JUM 1 Total Hydrocarbons (THC)
July 1, 1997
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
System Calibration
-0.2
85.7
270.9
461.8
Calibration Error
0.22%
0.22%
0.12%
0.11%
Correlation
Slope
Intercept
0.999988
0.9959296
0.9197352
15:57
Run 1
162.1
Corrected 161.1 ppm THC |
Ambient Air
16:10
July 2, 1997
1.7
Post Cal
0.8
-0.2
270.9
Drift
0.00%
0.00%
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
System Calibration
-0.2
85.7
272.8
463.7
Calibration Error
0.22%
0.14%
0.24%
0.17%
Correlation 0.999985
Slope 1.0007648
Intercept 0.8811314
13:57
Run 2
162.1
Corrected 160.3 ppm THC
Ambient Air
14:10
1.7
Post Cal
0.8
-0.2
272.8
Drift
0.00%
0.00%
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
System Calibration
-0.2
85.7
274:7
465.6
Calibration Error
0.21%
0.07%
0.37%
0.23%
Correlation
Slope
Intercept
0.9999772
1.0055999
0.8425275
33*53?* lte:
-------
LASCO
Styrene Bag Standards
JUM 1 Total Hydrocarbons (THC)
15:21 Run 3
Ambient Air
15:40
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
102 ppm Styrene
143.1 ppm Styrene
250.7 ppm Styrene
16:45
Calibration Gases
0.0 ppm
270.5 ppm
463.3 ppm
886.7 ppm
17:42 Run 4
Ambient Air
17:53
18:39 RunS
Ambient Air
322.50 (
1.7 0.9
Post Cal -0.2
467.5
System Calibration
-0.2
85.7
274.7
467.5
Correlation 0.9999908
Slope 1 .0094522
Intercept 0.5298777
255.6
295.7
414.1
Post Cal -0.20
274.70
System Calibration
-0.4
270.7
465.5
889.3
Correlation 0.9999988
Slope 1.0036288
Intercept -0.3201208
446.4
3.5 3.8
Post Cal -0.4
457.8
862.5
3.5 3.8
:orrected 319.0 ppm THC
Drift 0.00%
0.38%
Calibration Error
0.14%
0.06%
0.22%
0.14%
Corrected 253.3 ppm THC
Corrected 293.2 ppm THC
Corrected 41 1 .0 ppm THC
Drift 0.00%
0.00%
Calibration Error
0.01%
0.05%
0.08%
0.03%
Corrected 441.3 ppm THC
Drift 0.00%
0.77%
Corrected 855.9 ppm THC
(
Page 2
-------
LASCO
Styrene Bag Standards
JUM 1 Total Hydrocarbons (THC)
18:55
Post Cal
-0.4
457.8
Drift
0.00%
0.77%
Calibration Gases
0 ppm
1737 ppm
2418 ppm
4507 ppm
System Calibration
-2
1755
2442
4523
Calibration Error
0.15%
0.11%
0.18%
0.14%
Correlation 0.9999895
Slope 1.0038526
Intercept 5.6571339
19:56
Run6
1277
Corrected 1266 ppm THC
20:03
Post Ca)
-2
2461
Drift 0.00%
0.38%
20:52
Run 7
2652
Corrected 2636 ppm THC
21:00
Post Cal
-2
2461
Drift 0.00%
0.38%
Calibration Gases
0 ppm
1737 ppm
2418 ppm
4507 ppm
System Calibration
-2
1735
2442
4504
Calibration Error
0.11%
0.12%
0.39%
0.16%
Correlation
Slope
Intercept
0.9999751
1.0004054
3.3722138
21:54
Run8
3988
Corrected 3983 ppm THC
22:06
Post Cal
-2
4504
Drift
0.00%
0.00%
Page 3
-------
450.0'
400.0
P
p 358.8
" 288.0
P £50
i
• ^™ 465.6 467.3 —•
322.9
274.7 f"
83.7
Anbicnt Air
1'7 -«.8 -fl.2 •*
-------
467.5
374.7
85.7
-0.2
HS'43 1S'44
Jl'97,13'42'34
15>45 15-46
15'47
jutn-2
15'48 15'49 15'50
15'51
(HH'MM)
414.1
293.7
235.6
250.7 ppn Styren* Standard
143.1 ppn Styr«n« Standard
102 ppn Styren* Standard
-8.2
1.7
f
I
'55 16'08
1 "37,15 '33 '09
16-03 16-10 16*15 16*20
JUM1-2
16>2S
16-30 16'35
(HH'MM)
I
I
f
467.3
274.7
65.7
-e.e
16'40
2 Jul'97,16136'88
16-43
16 '50
16'93
-------
889.3
446.4
457.8
-e.4
Anbifnt flir
3.3
-8.4
17=10 17'13 17 = 88 17=35 17 = 30 17 = 35 17=40 17=45 17=53 17=55
Fppn a .Xii'97.17 = 06=41 JUM1-3 KII)
I
I
p
fc
£88. (
P'™
p 708.8
-
A :88.e
N
iee.9
e.e
863.5
3.3
• 18=28 18=25 18-30 18=35 18=48 18*45
- ppn a Jui'97.i8=a0'88 JUH1-3
457.8
-8.4
18 = 50 18 = 55 19 = 00
(HH'MM)
-------
4800'
3500
3008
2500
2000
1508
leoe
500
g
ppm
4523
2442
19'58
2 Jul'97, 19 '46 '25
1733
-2
19'55
1277
28 '88
JUI11-4
1
2461
-2
-2
20.85 c«'18
4508'
4800
3300
3000
2309
2800
1300
looe
500
8
20
an
L
'*> , •
-2
2461
-2
2632
-2
2461
-2
48 20>45 28>S8 29 '55 21>00 21 '05 21<10
3 Jul'97. 20 '40 -68 JUH1-4
4000.
3300
3000'
2300
2008
1300
1000
300
0
1
3988
2442
1738
-a
.^
4304
-a
21-43
21'33
,80
£3*89
22'18
-------
LASCO
Styrene Bag Standards
JUM 5 Total Hydrocarbons (THC)
July 1,1997
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
System Calibration
-0.2
85.7
276.6
467.5
Calibration Error
0.20%
0.01%
0.49%
0.28%
Correlation 0.9999647
Slope 1.010435
Intercept 0.8039237
15:57 Run 1 162.1 Corrected 156.9 ppm THC
Ambient Air 3.6 2.8
16:10 PostCal -0.2 Drift 0.00%
274.7 0.38%
July 2. 1997
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
System Calibration
-0.2
85.7
272.8
465.6
Calibration Error
0.15%
0.14%
0.10%
0.08%
Correlation 0.9999943
Slope 1.0046171
Intercept 0.5684815
13:57
Run 2
160.2
Corrected 157.8 ppm THC
Ambient Air
14:10
1.7
Post Cal
1.1
-0.2
272.8
Drift
0.00%
0.00%
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
System Calibration
-0.2
85.7
270.9
461.8
Calibration Error
0.22%
0.22%
0.12%
0.11%
Correlation 0.999988
Slope 0.9959296
Intercept 0.9197352
Pagel
-------
LASCO
Styrene Bag Standards
JUM 5 Total Hydrocarbons (THC)
15:21 Run 3
Ambient Air
15:40
Calibration Gases
0.0 ppm
84.1 ppm
270.5 ppm
463.3 ppm
102 ppm Styrene
143.1 ppm Styrene
250.7 ppm Styrene
16:45
Calibration Gases
0.0 ppm
270.5 ppm
463.3 ppm
886.7 ppm
17:42 Run 4
Ambient Air
17:53
18:39 RunS
Ambient Air
316.7 (
1.7 0.8
Post Cal -0.2
459.9
System Calibration
-0.2
83.8
270.9
459.9
Correlation 0.9999839
Slope 0.9938695
Intercept 0.3909664
249.9
290.0
408.4
Post Cal -0.20
270.90
System Calibration
-0.4
266.9
461.6
885.5
Correlation 0.9999934
Slope 0.9999279
Intercept -1 .6958077
434.9
3.5 5.2
Post Cal -0.4
457.8
839.6
-4.2 -2.5
lorrected 316.3 ppm THC
Drift 0.00%
0.38%
Calibration Error
0.12%
0.03%
0.34%
0.19%
Corrected 250.0 ppm THC
Corrected 290.3 ppm THC
Corrected 409.1 ppm THC
Drift 0.00%
0.00%
Calibration Error
0.13%
0.19%
0.00%
0.06%
Corrected 431.4 ppm THC
Drift 0.00%
0.38%
Corrected 843.9 ppm THC
Page 2
-------
LASCO
Styrene Bag Standards
JUM 5 Total Hydrocarbons (THC)
18:55
Post Cal
-8.0
434.9
Drift
0.76%
2.67%
Calibration Gases
0 ppm
1737 ppm
2418 ppm
4507 ppm
System Calibration
-2
1697
2423
4504
Calibration Error
0.22%
0.59%
0.29%
0.07%
Correlation
Slope
Intercept
0.9999419
1.0015077
-13.264862
19:56
Run 6
1239
Corrected 1250 ppm THC
20:03
Post Cal
-2
2385
Drift
0.00%
0.76%
20:52
Run 7
2633
Corrected 2642 ppm THC
21:00
Post Cal
-2
2385
Drift 0.00%
0.76%
Calibration Gases
0 ppm
1737 ppm
2418 ppm
4507 ppm
System Calibration
-2
1697
2404
4523
Calibration Error
0.39%
0.55%
0.11%
0.27%
Correlation
Slope
Intercept
0.9999354
1.005317
-21.513995
21:54
Run 8
4103
Corrected 4103 ppm THC
22:06
Post Cal
-2
4504
Drift
0.00%
0.38%
Page 3
-------
j.e
j.e
a.e
3.0
3.0
a.e
3.0
a.e
a.e
0.0
n
467.5
I!
376.6
83.7
15-50
1 Ail '97, 15*46 '36
-e.2
162.1
3.6 Anbient air
-0.2
374.7
15'55 16 = 08 16=05 16=10
JUHS-1
a.e
e.e
e.e
e.e
e.e
10.0
;a.e
19.0
;0.0
a.o
13
*^^^
465.6
P79
85
£72.8
160.2
7
~e'2 1.7 ftmbient ftir
-n.2
•BO 13=10 13'£0 13 '30 13 '48 13 = 50 14 = 00 14=10 14 = 2
m a Jui -97.13 =39 -34 JUM5-2
.0
.0
.0
.0
.0
.e
.0
.0
.0
1.7 Anbimt lir
•^^•~
461.8
270.9
M^
-A.P -a.e
»*,.,. •*rT1?<,eSn,ni IS'18 IS'15 l
459.9
316.7
-e.a
3'W ,13'85 I3i38 19>39 13-48
-------
1 — — I
83.8
L
1 -0.2
|450.0
488.8
338.8
£•50.8
130.0
108.8
58.8
0.0
IS-42 15'43 ~ f5^44
ppm 8 .ia'97,13'41'48
15--45
15*46 15'47
juns-z
15'48 15'49
CHH'WI)
450.8
400.8
338.0
^
£38.0
£«a.e
138.0
108.0
se.e
e.e
apm
849.9
298.0
488.4
_^^—^^^^—
250.7 ppn Styrene Standard
143.1 ppn Styrene Standard
183 ppn Styr«n« Standard
13'
2 ,
'34.88
16'18
...
JUM5-2
1.7
16-30 16'35
(HH'MM)
sea.e
430.8
488.0
cse.a
sse.e
£68.8
K-
lee.e
se.e
e.e
1.7
463.7
270.9
83.8
-e.e
16*40
16>49
-------
o
1
a
9
e
ieee.0
£88.8
700.0
500.0
480.0
£00.0
188.0
8.0
885.5
461.6
434.9
457.8
266.9
-0.4
3.S Art lent air
-0.4
17-10 17-15 17-20 17-25
ppm 2 -Xjl'97.17-07-17
17'30 17-35
JUMB-3
17^40 17-45
17-50
17-55
(HH'MM)
0
1
see. a
700.0
£00.0
400.0
£08.8
100.0
0.0
PP"«
. „•-.' •
-4.2 ftnbimt air
839.6
'
J
434.9
-8.0
18-38 18*35 18 '48 18-45 18-50 18-55 19 '80
Z Jul'97.18-23'26 JUH5-3 (HH'MM)
-------
4508-
4000
3500
3008'
2508
8000
1308
1008
soe
a
4504
2423
1697
-2
19<58 i9'55
pn 3 Jul'97,19'46.58
1339
£8" 08
JUM5-4
I,
-2
£383
-S
2B>85 28' IB
nn>
4000'
3500
3800
2300
2000
psoo
1000
500
0
-
1
,4103
2404
1697
-e
-e
^
4504
El'43
21'SB
-------
APPENDIX D
QA/QC DATA
-------
CALIBRATION PROCEDURES AND RESULTS
All of the equipment used is calibrated in accordance with the procedures
outlined in the Quality Assurance Handbook for Air Pollution Measurement
Systems. Volume III.* The following pages describe these procedures and
include the data sheets.
*EPA 60074-77-027b
-------
Pitot Tube Calibration
Each pitot tube used in sampling meets all requirements of EPA Method
2, Section 4.1.* Therefore, a baseline coefficient of 0.84 is assigned to each pitot
tube. The following pages show the alignment requirements of Method 2 and the
Pitot Tube Inspection Data Sheet(s) for each pitot tube used during the test
program.
*40 CFR 60, Appendix A, July 1995
-------
TRANSVERSE
TUBE AXIS
LONGITUDINAL
TUBE AXIS I
FLOW
(d)
81
(0
82 (* or -)
Bl (* or -)
0 A
(f)
Y
B
_ that can reautt freni field
"°" ot Type S Pttot tubes. These will not affect Cp as long «•
are
-------
TRANSVERSE
TUBE AXISv
\
FACE
•"• OPENING -
PLANES
(a) ENOVIEW
0.48 cm < 0. < 0.95 cm
(3/16 In.) w (3/8 In.)
A-SIDE PLANE
LONGITUDINAL
TUBE AXIS (
J
\
{
0.
t
A
B
' ' ''*•
J j
"S.
^s >
, PA
t
B-SIDE PLANE
(b)
NOTE:
D. < P < 1-50 Ot
PA= PB
€
A or 6
> «^M
(O
Property constructed Type S pttot tubes shown In: (a) end view, fa
opening planes perpendicular to transverse axis; (b) top view, face opening plans*
parallel to longitudinal axis; (e) side view, both legs equal length and ceiiieillnem
coincident when viewed from both aides. Baseline coefficient values of 0.84 may
be assigned to pilot tubes constructed this way.
-------
Dry Gas Meter and Orifice Meter
Dry gas meters and orifices are calibrated in accordance with Section 3.3.2
of the QA Handbook. This procedure invoives direct comparison of the dry gas
meter to a reference dry test meter. The reference dry test meter is routinely
calibrated using a liquid displacement technique. Before its initial use in the
field, the metering system is calibrated over the entire range of operation. After
each field use, the metering system is calibrated at a single intermediate setting
based on the previous field test. Acceptable tolerances for the initial and final
dry gas meter factors and orifice calibration factors are ±0.02 and ±0.20 from
average, respectively.
-------
POSTTEST DRY GAS METER CALIBRATION
MB#: 14
DATE: 5-30-97
PLANT: LASCO
RUN1
VACUUM ("Hg) 3.00
H("H20) 1.80
INITIAL RTM 981.918
FINAL RTM 989.945
INITIAL DGM 21.881
FINAL DGM 30.254
TEMP. RTM (F) 78.0
TEMP. DGM (F) 84.0
TEST TIME (MIN.) 11.0
BAROMETRIC PRE 29.63
PERFORMED BY: g gay
PRETEST Y : 0.966
PRETEST H@: 1.862
(in. hg.)
RUN 2
3.00
1.80
989.945
997.908
30.254
38.654
78.0
84.0
11.0
RUN 3
3.00
1.80
997.908
1007.591
38.654
48.609
78.0
84.0
13.0
NET VOLUME RT 8.027 7.963
NET VOLUME DG 8.373 8.400
Y 0.965 0.954
H@ 1.924 1.955
PRIOR Y = 0.966
RECHECK Y = 0.966
% DIFFERENCE = 0.017
AVERAGE H@= 1.909
Y = (Vw x Pb x (Td + 460)) / (Vd (Pb + (dHd / 13.6))x(Tw + 460)
H@ = 0.0317 x H / (Pb (Td + 460)) x ((Tw + 460) x time) / Vw)A2
9.683
9.955
0.979
1.847
-------
DRY GAS AND ORFICE CALIBRATION
CONTROL BOX N MB-14
DATE: 26DEC96
Hd ("H2O)
VACUUM ("HG)
INITIAL WTM
FINAL WTM
INITIAL DGM
FINAL DGM
TEMP. WTM (F)
TEMP. DGM (F)
TEST TIME (MIN.)
NET VOLUME WT
NET VOLUME DG
Y
H@
RUN1
0.50
10
421.973
433.978
440.708
453.247
69.0
76.0
30.0
12.005
12.539
0.969
1.756
RUN 2
0.75
10
434.239
445.767
453.623
465.763
68.0
78.0
24.0
11.528
12.140
0.966
1.814
BAROMETRIC PRESS
PERFORMED BY :
RUNS
1.00
10
446.842
458.269
466.990
479.076
68.0
81.0
21.0
11.427
12.086
0.966
1.875
RUN 4
1.50
10
458.765
470.085
479.502
491.468
69.0
82.0
17.0
11.320
11.966
0.966
1.881
29.43
B.FISHER
RUNS
2.00
10
470.449
481.847
491.855
503.912
69.0
83.0
15.0
11.398
12.057
0.966
1.923
RUN 6
4.00
10
483.036
494.839
505.180
517.635
69.0
85.0
11.0
1 1 .803
12.455
0.967
1.922
AVERAGE Y = 0.966
ACCEPTABLE Y RANGE =
AVERAGE H@= 1.862
ACCEPTABLE dH@ RANGE =
0.946
TO
1.662 TO
0.986
2.062
Y = (Vw x Pb x (Td + 460)) / (Vd (Pb + (dHd /13.6)) x (Tw +460))
H@ = 0.0317 x Hd / (Pb (Td + 460)) x (((Tw + 460) x time) / Vw)A2
-------
Pacific Environmental Services VOST Box Calibration
Date: 3JAN97 Flow Rate: 0.5 I/min
Vost Box Number: V-l Rotameter Setting: 0.6
Bubble Meter Temp. : 70
Run 1
Bubble Meter
0.4994 0.4996
0.4994 0.4997
0.4995 0.4995
0.4997
Average: 0.4995429
Run 2
Bubble Meter
0.5 0.4998
0.4998 0.5003
0.5002 0.4998
0.5
Average: 0.4999857
Run 3
0.5 0.5003
0.5002 0.4998
0.5002 0.5003
0.5004
Average: 0.5001714
Meter Box
Initial volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y=
7512.5
7518.5
84
85
84.5
11.43
0.5109554
0.9776643
7519.5
7525.5
85
86
85.5
11.38
0.5122596
0.9760397
7526
7532
86
87
86.5
11.38
0.5113223
0.9781922
Average Y= 0.9772987
-------
Pacific Environmental Services VOST Box Calibration
Date: 6/9/97
Vost Box Number: V-l
Run 1
Bubble Meter
146.5 146.1
146.4 146.2
146.1 146.3
146.3
Average: 146.27143
Run 2
Bubble Meter
145.7 146.3
145.9 146.3
145.2 146.3
146.2
Average: 145.98571
Run 3
145.7 . 145.9
145.6 146
145.7 146.1
146.2
Average: 145.88571
Flow Rate:
Rotameter Setting:
Bubble Meter Temp. :
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y=
ISOcc
.20 L/min
70
8049
8052
81
82
81.5
19.858
0.1478642
0.9892279
8052
8056
82
83
82.5
27.445
0.1423878
1 .0252682
8056
8059
83
84
83.5
19.68
0.1486526
0.981387
Average Y= 0.9986277
-------
Pacific Environmental Services VOST Box Calibration
Date: 2JAN97 Flow Rate: 0.25/min
Vost Box Number:. V-2 Rotameter Setting: 0. 19
Bubble Meter Temp. : 68
Run 1
Bubble Meter
0.2523 0.2515
0.2515 0.2511
0.2505 0.2505
0.2515
Average: 0.2512714
Run 2
Bubble Meter
0.2517 0.2505
0.2502 0.2504
0.2496 0.2503
0.2504
Average: 0.2504429
Run 3
0.2513 0.2521
0.252 0.25
0.251 0.2508
0.251
Average: 0.2511714
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
1754.7
1757.7
82
84
83
11.29
0.2583815
0.9724823
1766.5
1769.5
87
87
87
11.03
0.2625381
0.9539296
1770.8
1773.8
87
88
87.5
11.25
0.2571689
0.9766787
Average Y= 0.9676968
-------
Pacific Environmental Services VOST Box Calibration
Date: 6/9/97
Vost Box Number: V-2
Bubble Meter
149.4 149.4
150 149.1
149.8 148.7
148.5
Average: 149.27143
Bubble Meter
149.5 149.4
149.5 149.3
149.4 149.2
148.9
Average: 149.31429
147.9 148.4
147.3 148.9
147.6 149.4
149.5
Average: 148.42857
Flow Rate:
Rotameter Setting:
Bubble Meter Temp. :
Run 1
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Run 2
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Run 3
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y=
150cc
.25 L/min
70
2491
2495
85.5
89
87.25
26.239
0.1476396
1.0110529
2495
2501
89
90.5
89.75
38.58
0.1499338
0.9958678
2509
2514
90.5
92.5
91.5
31.833
0.1509464
0.9833197
Average Y= 0.9967468
-------
Pacific Environmental Services VOST Box Calibration
Date: 2JAN97 Flow Rate: 0.25/min
Vost Box Number: V-3 Rotameter Setting: 0.22
Bubble Meter Temp. : 68
Run 1
Bubble Meter
0.2523 0.2513
0.2519 0.2516
0.2514 0.2514
0.2514
Average: 0.2516143
Run 2
Bubble Meter
0.2489 0.2491
0.2492 0.2495
0.2488 0.2492
0.2491
Average: 0.2491143
Run 3
0.2478 0.2481
0.2479 0.2484
0.2479 0.2482
0.2482
Average: 0.2480714
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
1034.3
1037.3
88
89
88.5
11.37
0.2539909
0.9906431
1041.3
1044.32
90
90
90
11.56
0.2507958
0.9932951
1045.5
1048.5
90
91
90.5
11.41
0.2521809
r= 0.9837042
Average Y= 0.9892141
-------
Pacific Environmental Services VOST Box Calibration
Date: 6/9/97
Vost Box Number: V-3
Bubble Meter
243 242.4
242.5 242.8
242.4 242.6
243
Average: 242.67143
Bubble Meter
239.9 239.4
240.3 239.8
240.1 240.1
240.2
Average: 239.97143
237.5 237.3
237.3 237.6
237.4 237.5
237.8
Average: 237.48571
Flow Rate:
Rotameter Setting:
Bubble Meter Temp. :
Run 1
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Run 2
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Run 3
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
.25 L/min
20
70
4900
4905
86
88
87
20.2
0.239832
1.0118391
4905
4910
88
90
89
20.6
0.2343184
1.0241256
4910
4915
90
90
90
20.57
0.2342334
1.0138848
Average Y= 1.0166165
-------
ENVIRONMENTAL SUPPLY COMPANY
2142 E. Geer Street, Durham, North Carolina 27704
(919) 956-9688 • FAX: (919) 682-0333
Date:
Model:
S/N:
DGMS/N:
4/9/97
UNI-VOS-110
1506
96205
Barometric Pressure (In Hg):| 29.75
Reference Meter
Type: American
Model: DTM-115
Ye: 1.000
UNI-VOS CONSOLE
REFERENCE METER
Rotameter
DGM
Initial
(liters)
DGM
Rnal
(liters)
Volume
Total
(liters)
DGM Temp.
Initial
("R
Rnal
CR
Average
Temp.
(°F)
.DGM
Pressure
(in HjO)
663.550
672.625
682.135
672.825
682.135
691.590
9.275
9.310
9.455
63
63
64
63
63
65
63
63
64.5
2.8
2.8
2.8
692.290
700.985
709.660
700.985
709.660
718.470
8.695
8.675
8.810
64.5
65
66
65.5
• 65
66
65
65
66
1.4
1.4
1.4
718.760
726.600
734.660
726.600
734.660
742.852
7.840
8.060
8.192
67
67.5
68
67.5
68
69
67.25
67.75
68.5
1
1
1
Volume Volume
Initial Final
(liters) (liters)
Volume
Total Temperature
(liters) (°F)
Yc Avg %deviation
1283.940
1293.935
1303.770
1293.935
1303.770
1313.710
9.995
9.835
9.940
66
66
66
1.064
1.043
1.041
1.049
-1.4%
0.6%
0.8%
1314.445
1323.715
1332.990
1323.715
1332.990
1342.263
9.270
9.275
9.273
66
66
66
1342.625
1351.442
1360.485
1351.442
1360.485
1369.720
8.817
9.043
9.235
66
66
66
1.060
1.063
1.049
1.125
1.123
1.130
1.058
. . -
1.126
-0.3%
-0.6%
0.8%
0.1%
0.3%
-0.4%
Calibration performed by:_
-------
Pacific Environmental Services VOST Box Calibration
Date: 6/4/97
Vost Box Number:
ES-1
Flow Rate:
Rotameter Setting:
Bubble Meter Temp.
.25 1/min
0.5
72
Run 1
Bubble Meter
244.4 245.8
244.5 246.2
244.9 246.2
Average: 245.33333
Run 2
Bubble Meter
250.2 250.3
250 251.2
251.5 250.2
Average: 250.56667
Run 3
259.6 259.5
258.9 260.1
259.3 260.4
Average: 259.63333
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y =
Meter Box
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM=
Y =
Initial Volume
Final Volume
Initial Temp.
Final Temp.
Average Temp.
Time:
QDGM =
Y=
1200
1205
81
82
81.5
20.93
234.70046
1.045304
1205
1210
82
82
82
20.74
236.63207
1.0588872
1210
1218
82
82
82
31.81
246.85314
1.0517724
Average Y= 1.0519879
-------
Digital Indicators for Thermocouple Readout
A digital indicator is calibrated by feeding a series of millivolt signals to the
input and comparing the indicator reading with the reading the signal should
have generated. Error did not exceed 0.5 percent when the temperatures were
expressed in degrees Rankine. Calibration data are included in the following
Thermocouple Digital Indicator Calibration Data Sheet(s).
-------
PACIFIC ENVIRONMENTAL SERVICES, INC.
DATE:
27-Dec-96
THERMOCOUPLE DIGITAL INDICATOR
CALIBRATION DATA SHEET
OPERATOR:
B. FISHER
CALIBRATION DEVICE: . D.y'4JL
INDICATOR NO.:
SERIAL NO.:
MANUFACTURER:
MB-14
TEST POINT
NO.
I
T
3
4
5
6
7
8
9
10
MILLIVOLT
SIGINAL
-0,692
1.520
3.819
6.092
8.314
10.560
22.251
29.315
36.166
42.732
EQUIVALENT
TEMP UF
0
100
200
300
400
500
1000
1300
1600
1900
DIGITAL INDICATOR
TEMP READING °F
0
101
203
302
399
499
999
1296
1596
1894
DIFFERENCE %
0
-0.18 ,
-0.45
-0.26
0.12
0.10
0.07
* 0.23
0.19
0.25
Percent difference must be less than or equal to 0.5 %
Percent difference:
(Equivalent temp..°R - Digital indicator tern. °R) * ( 100%)
(Equivalent temp, °R)
Where °R = "F + 460
DIGITAL INDICATOR
-------
Stack Thermocouples
Each thermocouple is calibrated by comparing it with an A5TM-3F
thermometer at approximately 32°F, ambient temperature, 100°F, and 500°F. The
thermocouple read within 1.5 percent of the reference thermometer throughout
the entire range when expressed in degrees Rankine. The thermocouples may
be checked at ambient temperature at the test site to verify the calibration.
Calibration data are included in the following Thermocouple Calibration Data
Sheet(s).
-------
PACIFIC ENVIRONMENTAL SERVICES,1NC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR STACK THERMOCOUPLES
DATE:
10-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR:
B.FISHER
THERMOCOUPLE NUMBER: T3A
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM 3F
Reference
point
number
1
2
3
4
Source"
(Specify)
Ambient Air
Cold Bath
Hot Bath
Hot Oil
Reference
Thermometer
Temperature,°F
70
32
182
406
Thermocouple
Potentiometer
Temperature,°F
70
31
182
407
Temperature
Difference,"
%
0.00
0.20
0.00
-0.12
Type of calibration used.
Vref. temp.8F+46QWtest thermometer temp.sF+46Ql
X100
reftemp,°F+460
100<1.5%
Comments:
STACK THERMOCOUPLE
-------
PACIFIC ENVIRONMENTAL SERVICES,1NC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR STACK THERMOCOUPLES
DATE:
LO-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR:
B.FISHER
THERMOCOUPLE NUMBER: T3B
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM3F
Reference
point
number
1
2
3
4
Source"
(Specify)
Ambient Air
Cold Bath
Hot Bath
Hot Oil
Reference
Thermometer
Temperature,°F
74
33
203
414
Thermocouple
Potentiometer
Temperature,°F
72
31
203
410
Temperature
Difference,"
%
0.37
0.41
0.00
0.46
Type of calibration used.
bfref. temp.flF+460Wtest thermometer temp.aF+460^
X100
reftemp,°F+460
100<1.5%
Comments:
STACK THERMOCOUPLE
-------
PACIFIC ENVIRONMENTAL SERVICES,1NC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR STACK THERMOCOUPLES
DATE:
10-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR: B.FISHER
THERMOCOUPLE NUMBER: T3C
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM3F
Reference
point
number
1
2
3
4
Source1*
(Specify)
Ambient Air
Cold Bath
Hot Bath
Hot Oil
Reference
Thermometer
Temperature,°F
70
32
183
398
Thermocouple
Potentiometer
Temperature,°F
70
31
184
400
Temperature
Difference,"
%
0.00
0.20
-0.16
-0.23
Type of calibration used.
"(ref. temp.flF+460Htest thermometer temp.flF+4601
reftemp,°F+460
Comments:
X100
100<1.5%
STACK THERMOCOUPLE
-------
PACIFIC ENVIRONMENTAL SERVICES,INC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR STACK THERMOCOUPLES
DATE:
10-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR:
B.FISHER
THERMOCOUPLE NUMBER:- T4C
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM3F
Reference
point
number
1
2
3
4
Source"1
(Specify)
Ambient Air
Cold Bath
Mot Bath
Hot Oil
Reference
Thermometer
Temperature,°F
71
38
179
385
Thermocouple
Potentiometer
Temperature,°F
70
37
178
390
Temperature
Difference,6
%
0.19
0.20
0.16
-0.59
Type of calibration used.
"fref. temo.°F+46QWtest thermometer temD.°F+460}
X100
reftemp,°F+460
100<1.5%
Comments:
STACK THERMOCOUPLE
-------
Dry Gas Thermocouples and Impinger Thermocouples
The dry gas thermocouples are calibrated by comparing them with an
ASTWI-3F thermometer at approximately 32°F, ambient temperature, and a higher
temperature between approximately 100° and 200°F. The thermocouples agreed
within 5aF of the reference thermometer. The impinger thermocouples are
checked in a similar manner at approximately 32°F and ambient temperature, and
they agreed within 2°F. The thermocouples may be checked at ambient
temperature prior to the test series to verify calibration. Calibration data are
included in the following Dry Gas Thermometer and Impinger Thermocouple
Calibration Data Sheet(s).
-------
PACIFIC ENVIRONMENTAL SERVICES,INC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR METER BOX
DATE:
27-Dec-96
AMBIENT TEMPERATURE: 70 °F
CALIBRATOR: B.FISHER
THERMOCOUPLE NUMBER:
BAROMETRIC PRES.(ln.Hg):
REFERENCE:
Mercury-in-glass:
Other:
MB-14
29.4
ASTM 3F
Reference
point
number
INLET
1
2
3
OUTLET
1
2
3
SourceJ
(Specify)
Ambient Air
Cold Bath
Hot Bath
Ambient Air
Cold Bath
Hot Bath
Reference
Thermometer
Temperature.°F
74
33
• 128
70
33
149
Thermocouple
Potentiometer
Temperature.°F
75
34
129
71
34
150
Temperature
Difference."
°F
1
1
1
1
1
1
"Type of calibration used.
Allowable tolerance ±5°F
Comments:
METER BOX
-------
PACIFIC ENVIRONMENTAL SERVICES.INC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR SAMPLE HEAD
DATE: 10-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR: B.FISHER
THERMOCOUPLE NUMBER:
SH-1
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM3F
Reference
point
number
1
2
Source"
(Specify)
Ambient Air
Cold Bath
Reference
Thermometer
Temperature,°F
70
32
Thermocouple
Potentiometer
Temperature,°F
72
32
Temperature
Difference,"
°F
-2.00
0.00
"Type of calibration used.
"Allowable tolerance ±2°F
Comments:
SAMPLE HEAD
-------
PACIFIC ENVIRONMENTAL SERVICES,INC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR SAMPLE HEAD
DATE: 10-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR: B.FISHER
THERMOCOUPLE NUMBER: SH-2
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM 3F
Reference
point
number
1
2
SourceJ
(Specify)
Ambient Air
Cold Bath
Reference
Thermometer
Temperature,°F
71
33
Thermocouple
Potentiometer
Temperature,°F
71
33
Temperature
Difference,"
°F
0.00
i
0.00
"Type of calibration used.
"Allowable tolerance ±2°F
Comments:
SAMPLE HEAD
-------
PACIFIC ENVIRONMENTAL SERVICES,INC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR SAMPLE HEAD
DATE:
IO-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR:
B.FISHER
THERMOCOUPLE NUMBER: SH-3
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM3F
Reference
point
number
1
2
SourceJ
(Specify)
Ambient Air
Cold Bath
Reference
Thermometer
Tempera ture,°F
72
32
Thermocouple
Potentiometer
Tempera ture,°F
72
32
Temperature
Difference,11
°F
0.00
0.00
"Type of calibration used.
"Allowable tolerance ±2°F
Comments:
SAMPLE HEAD
-------
PACIFIC ENVIRONMENTAL SERVICES,!NC.
TEMPERATURE SENSOR CALIBRATION DATA FORM
FOR SAMPLE HEAD
DATE:
IO-Dec-96
AMBIENT TEMPERATURE: 70
CALIBRATOR: B.FISHER
THERMOCOUPLE NUMBER:
SH-4
BAROMETRIC PRES.(ln.Hg): 29.09
REFERENCE:
Mercury-in-glass:
Other:
ASTM 3F
Reference
point
number
1
2
Source"1
(Specify)
Ambient Air
Cold Bath
Reference
Thermometer
Temperature,°F
71
33
Thermocouple
Potentiometer
Temperature,°F
71
33
Temperature
Difference,"
°F
0.00
0.00
Type of calibration used.
"Allowable tolerance ±2°F
Comments:
SAMPLE HEAD
-------
Trip Balance
The trip balance is calibrated by comparing it with Class-S standard
weights, and it agreed within 0.5g. Calibration data are shown in the following
Trip Balance Calibration Data Sheet(s).
-------
_
?5Cate
3-26 Whitney Drive. Milford Ohio 45150 • 513-576-0700
3 3570 intercity Drive, Dayton. Ohio 45424 • 037-236-6748
3 6314 Seeds Road. Grove City, Ohio 43123 • 514-871-46-16
SERVICE ORDER
.03 NO,
I
I
7 ' 1 "^ I U 1
DATE k- • * ' ' i
PERSON CALLING .
PHONE *
CUSTOMER
n L , a "I - ,7
^ ~ / - -
AOO
WHE
WAN
SER
EOU
CON
1
2
3
4
ZIP { •
RESS ;?00 DUKE DRIVE cr1ITE 150 CITYA^TATP i4ASON °H CODE islik1™
N SERVICE WHEN CALL
TED PROMISED TAKEN BY ML
VICE REQUEST
IPMENTTYPE: •-
DITION FOUND WHEN TECHNICIAN AH
Scale No. 0
MANUFACTURER
4 /v • '.
,-\Sr
- M
•
BIVFQ
i$9 Location
I.
MODEL -
'•: r - ? .- - ••
CT- ^X^o^
^ P - « ° T
SERIAL NUMBER
. C 0 L^l 1 IV
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uvooi7o
C^ C3Z^t-
CAPACITY |
/6(J ^ » OL*J t r,-*-.
/20UJC . ( rrnB
I
SERVICE PERFORMED/RECOMMENDATIONS:
0 ~ - - - r : ;.. ,j f. .... ,
t
_£
*• %*-" .^'i- ^/C.
..- "Cue Qj3€<-c.i.'L .- 4 C
t
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DESCRIPTION OF PARTS USED
-------
r
SCIALTY
722 S. WENTwORTH AVENUE
CCAGO, IL 60628
Certificate of Analysis - EPA Protocol Gas Standard
Page 1 of 1
LFORMED ACCORDING TOEPA TRACEABILITY PROTOCOL FOR ASSAY AND CERTIFICATION OF GASEOUS CALIBRATION STANDARDS (PROCEDURE
itomeri
iIR PRODUCTS AND CHEMICALS, INC.
.822 INDUSTRY LANE
DI BUSINESS PARK
URHAM NC 27709
O: Rel;
Certified Concentration * * *
4 Certified
ponent Concentrat ion
PANE
/Cl)
t747-01
Order No? 833-071,
Batch No: 861-30888
Notes:
Cylinder No: SG9133829BAL
Cylinder Pressure*: 2000 psig
Certification Date: 02/27/96
Expiration Date: 02/27/99
********* Reference Standards ********* ************* Analytical Instrumentation *************
Standard Instrument Serial Last Measurement
Cylinder_# Number Concentration Make/Hodul Number Calibration Principal
30.4000 PPM Gow-Mac 750
31.4 tO.25 PPM SG9128572BAL GMIS
59405U 02/08/96 GC-FID
ance Gas; AIR
jen Concentration
19.9 %
| Standard should not be used below 150 psig
Approved By:
Richard >ry
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STREET. TROY, Ml 48083
(810)589-2950 FAX:(810) 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENVIRONMENTAL SER
ATTN: GARY GUY
4700DUKEDRIVE,STEI50
MASON, OH 45040
ANALYTICAL INFORMATION
Assay Laboratory
Scon Specialty Gases, Inc
1290Combermere
Troy, MI 48083
Purchase Order : 103-97-0073
Scott Project #: 504488
This certification was performed according to EPA Traceabiliry Protocol For Assay and Certification ot Gaseous
Calibration Standards: Procedure GI: September, 1993.
Number : ALM060872
Pressure + : 2000 psig
r
Certificate Date : 11/14/96 Expiration Date :
Previous Certificate Date : None
11/14/99
Components
Propane
Certified Concentration
49.37 ppm
Analytical Uncertainty*
±1% NIST Directly Traceable
Balance Gas: Air
+Do not use when cylinder pressure ii below 150 pjig.
'Analytical accuracy n inclusive of usual known error sources which at lean include prccnion of the measurement processes.
REFERENCE STANDARD
J5K..«.*^ Eipiration Date
' ^*-SRM2643A 7/24/99
Cylinder Number
SX20435
Instrument/Model/Serial #
C3H8: Varian/1400/08982426
Last Date Calibrated
11/14/96
Concentration
99.1 ppm Propane in Nitrogen
Analytical Principle
Gas Chromatography
'"•;.*»(•«? ^ANALYZER READINGS (Z-ZeroCas R-Referenee Gas T-TestGas r-Correlarion Coefflcleoc) ^
First Triad Analysis Second Triad Analysis Calibration Curve
OMK11/14/M RMponw Unite mv
Z1O.OO R1M62.30 T1-229.40
R2MBX30 Z2-0.00 TM28.40
Z3^).00 T3420.40 R3M82.30
Axo. Cone, of CUM. C A 49.37 ppm
l«1.00000
0*0.000000000 f- ^r^onououutift
"•^
"-^saHr-.^
i; ^'**1'V-*i:^" * *"
fcV- •*jS.-5.iy'l-1-
-------
Scott Specialty Gases, Inc.
1 /3J tAST CLUB BOULEVARD, DURHAM. NC '2/AM
(919)Z2LH£U3
CERT1RCATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
Mr. Bill Buynitzky
Deeco, Inc.
203 North Harrison Avenue
Cary.NC 27513
Assay Laboratory
Scott Specialty Gases, Inc.
1750 East Club Boulevard
Durham, NC 27704
Purchase Order 0221940930-WDB
Scott Project # 12-06571
ANALYTICAL INFORMATION
Certified to exceed the minimum specifications of EPA Protocol Procedure #G1, Section Number 3.0.4
Cylinder Number ALM-031639 Certification Date 03-22-94 Expiration Date 03-22-97
Cylinder Pressure 2000 PSIG Previous Certification None
ANALYZED CYLINDER
Components Certified Concentration Analytical Uncertainty'
Propane 49.8 PPM +/- 1% N1ST Directly Traceable
Air . Balance
•Analytical uncertainty is inclusive of usual known error sources which al least includes reference standard error & precision of the measurement processes.
REFERENCE STANDARD
Type Expiration Date
GM1S 03-28-94
Cylinder Number
K003986
Concentration
96.3 PPM Balance in Nitrogen
INSTRUMENTATION
Instrument/Model/Serial #
Varian/3400/0160
Last Date Calibrated
02-26-94
Analytical Principle
Gas Chromatography
ANALYZER READINGS (Z=Z«roGas Reference Gas T=TestGa» r-Corrdation Coefficient)
Components
Propane
First Triad Analysis Second Triad Analysis
Date: 03-22-94 Respoaso Units: Area
STD-63002S SPL-327477
SPL-32S102 SPL-32JOOI
STO-«32703 STD-«4833
Data: Response Units:
STD- SPL-
SPL- SPL-
STD- STD-
Date: Retpome Uoia:
STO- SPL-
SPL- SPL-
STD- STD-
Date: Reapome Units:
STD- SPL-
SPL- SPL-
STD- STD-
Date: Response Units:
STD- SPL-
SPL- SPL-
STD- STD-
Date: Respoase Units:
STD- SPL-
SPL- SPL-
STD- STD- —
n
\J
(
Calibration Curve
Date: 02-26-94
Date:
1 A «* t lA^kAll.
vfi^wv^'^aY ^^% v^a^^'^a' \A*
Analyst A. Barber
-------
Scott Specialty Gases, Inc.
1750 EAST CLUB BOULEVARD, DURHAM, NC 27704
(919) 22WB03 FAX (919) 220-0806
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
Mr. BUI Buynitzky
Deeco, Inc.
203 North Harrison Avenue
Cary.NC 27513
ANALYTICAL INFORMATION
Assay Laboratory
Scott Specialty Gases, Inc.
1750 East Club Boulevard
Durham, NC 27704
Purchase Order 0221940930-WDB
Scott Project # 12-06571
Certified to exceed the minimum speciGcations of EPA Protocol Procedure #G1, Section Number 3.0.4
Cylinder Number ALM-009890 Certification Date 03-21-94 Expiration Date
Cylinder Pressure 2000 PSIG Previous Certification None
03-21-97
ANALYZED CYLINDER
Components Certified Concentration Analytical Uncertainty*
Propane 86.6 PPM +/-1% N1ST Directly Traceable
Air jj Balance
'Analytical uncertainty a inclusive of usual known error sources which at least includes reference standard error & precision of the mea«uremenl processes.
REFERENCE STANDARD
Type Expiration Date
GMIS 03-28-94
INSTRUMENTATION
Instrument/Model/Scrial #
Varian/3400/0160
Cylinder Number
K-003986
Last Date Calibrated
02-26-94
Concentration
96.3 PPM Balance in Nitrogen
Analytical Principle
Gas Chromatography
ANALYZER READINGS (Z=ZeroGaa R=Referen« Gas T=T*stGas r=C'orrelndon Coefficient)
Components
Propane
First Triad Analvsis
Second Triad Analysis
Calibration Curve
Date: 03-21-94
STD-6307S1
SPL-5671M
STD-479913
Response Units: Area
SPL-366170
SPL-568689
STD-630913
Date:
STD-
SPL-
STD-
Refponse Units:
SPL-
SPL-
STD-
Date: 02-26-94
Date:
STD-
SPL-
STD-
Response Itniu:
SPL-
SPL-
STD-
Date:
STD-
SPL-
STD-
Retponse Units:
SPL-
SPL-
STD-
Date:
Date:
STD-
SPL-
STD-
ResponH Unita:
SPL-
SPL-
STD-
Date:
STD-
SPL-
STD-
Rnpoaa Units:
SPL-
SPL-
STD-
Date:
Analyst A. Barber
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STRfelY,TROY, MI 48083
AX!(B 10') 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENVIRONMENTAL SER
ATTN: GARY GUY
4700 DUKE DRIVE. STE 150
MASON, OH 45040
Assay Laboratory
Scott Specialty Gases. Inc
!290Combermere
Troy, Ml 48083
Purchase Order: 103-97-0143
Scott Project #: 509412
ANALYTICAL INFORMATION
This certification was performed according to EPA Traceability Protocol For Assay and Certification of Gaseous
Calibration Standards; Procedure GI. September, 1993,
Certificate Date: 3/31/97 Expiration Date: 3/31/2000
Previous Certificate Date : None
Number: ALMOI0756
''CjfHnder Pressure + : 1900 psig
7»
'.' ANALYSED CYLINDER
Component;
Propane
Certified Concentration
83.67 ppm
Analytical Uncertainty*
±1% NIST Directlv Traceable
Balance Gas; Air
+Do not use when cylinder prcustut is below I SO pitg.
'Analytical aecuftcv u inclusive ol usual known error sources which at le»M include precision ol >he meaiurenienl proceues.
REPr.RKNrr.r~
Espiration Date
8/5/98
Cylinder Number
ALM032007
Concentration
95.5 ppm Propane in Air
. , , .
;_,>l*i' *,.. • INSTRUMENTATION
Insirument/Model/Serul K
. C3IB: Varian/1400/08982426
Last Date Calibrated
3/31/97
Analytical Principle
Gas Chromatography
ANALYZER READINGS (Z-ZcroGas R-RefercnceGai T°TestG«s r-Correlirion Coefficient!
.v -,*••• i,«; j. Components
Propane
"
First Triad Analysis
Second Triad Analysis
Calibration Curve
D*« MIST RMpom*Un«K m»
21-0.00 R1«4,734.00
TJM.147.00
R2-4.734.CX3 22^.00 T2M.14fl.00
Z3*0,OQ n«4.14700
83.87 Bern
CoM«ftcmioiiiA*i
f«100000 NTMI18H
CotvttMitK A^HQLOQECKMflflB
p«0 .QQQQQCrOOO ^^?. 000000000
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STREET. TROY, Ml 48083
(810) 589-2950 FAX:(810) 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENVIRONMENTAL SER
ATTN: GARY GUY
4700 DUKE DRIVE. STE 150
MASON, OH 45040
ANALYTICAL INFORMATION
Assay Laboratory
Scon Specialty Gases. Inc
l290Combermere
Troy, Ml 48083
Purchase Order: 103-97-0073
Scott Project #: 504488
This certification was performed according to EPA Traccability Protocol For Assay and Certification ot Gaseous
'.Calibration Standards; Procedure Gl: September, 1993.
nderNumber: ALM028660
Pressure*; 2000 psig
CYLINDER
Propane
Certificate Date : 11/14/96
Previous Certificate Date : None
Certified Concentration
84.08 ppra
Expiration Date : 11/14/99
Apalvtical Uncertainty*
±1% NIST Directly Traceable
.:•; Balance Gas: Air
• *'•**,/ ^-' ' :
•'*'?& *:+wai not rat wbeo eyliader presisuit ii below ISOpsig.
. :J~ - .*An»)yncjJ acoincv n inclusive ol usual known error sources which at least include precision of the measurement processes.
STANDARD
Expiration Date
7/24/99
Cylinder Number
SX20435
Concentration -"jv
99.1 ppm Propane in Nitrogen
- *'-" PiSTRUMENTATIO^
hutrument/Model/Seria) #
. -IOH8: Varian/1400/08982426
'
Last DaU Calibrated
11/14/96
Analytical Principle
Gas Chromatography
'**sw .^.^^ANALYZER READINGS (Z-Zere Gaa R-Referetiee Gas T-Ttst Gas r-Correiation Coefficient)
*2* *-.^^^^ ^TJ'^.^rc^;] _u i ni_-m JILJ -t __.^^________^_____^_^^_Jiiiii.—.^
First Triad Analysis Second Triad Analysis Calibration Curve
0«t»: 11/1*96 R««pon»»Ontr mv
Z1KI.OO R1-482JO T1O82.W
R2M62.30 Z2«O.OO T»4B2.aO
23*0.00 T3-390.10 R&M82.30
Avg. Cone, ol CIML Cyl 84.08 ppm
(-100000
WOW3A
B«> 213518200
oo ooooooooo
e«oonooa:ir«)
•*..-••* -T-"«r- -Jc"1
wv
mm^'^-m^^m^• • • ' " "•• .itfv*1^ s •' • '^V^'Wr
^y&il'i^fcfS^^ '"^^l^'^t
h':«^J»tt.^jV¥?'3!.'.*,^s^J?3^Jf^Kii:'#iV«r.- - '.A*;--?*- --.atS^ifMt •'•: :^*.: 3&3ire
?Kpr
&H**
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STREET, TROY, Ml 48083
(810)589-2950 FAX:(810) 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENVIRONMENTAL SER
ATTN: GARY GUY
4700 DUKE DRIVE, STE 150
MASON, OH 45040
Assay Laboratory
Scott Specialty Gases, Inc
1290Combermere
Troy, MI 48083
Purchase Order: 103-95-0238
Scott Project # : 578642
ANALYTICAL INFORMATION
This certification was performed according to EPA Traceability Protocol For Assay and Certification of Gaseous
Calibration Standards: Procedure Ul: September, 1993.
Cylinder Number: AAL710
. Cylinder Pressure + : 1900 psig
Certificate Date: 3/17/95
Previous Certificate Date : None
Expiration Date: 3/17/98
ANALYZED CYLINDER
Component!
Propane
Certified Concentration
270.5 ppm
Analytical Uncertainty*
±1% NIST Directly Traceable
Balance Gas: Air
+Do DM use when cylinder preunire ii below 150 piig.
'Analytical accuracy i» inclusive of usual known error source* which at leail include precnion of the measurement processes.
REFERENCE STANDARD
•l''5r/c- JS*P*
' „ ^ RTTRM
' ''
Expiration
1668' 6/7/96
Cylin«Vr Number
ALM-032015
Concentration
95.5 ppm Propane in Air.
.
INSTRUMENT ATTON
Lutrument/Model/Serial tt
rVop:Beckman/400/l002059
Last Date Calibrated
2/22/95
Analytical Principle
Flame lonization Detection
. ^.
ANALYZER READINGS (Z-ZeroGas R-Refcreoee Gas T-TestGas r-CorreUtion Coefficient)
^%*£*
••-t?4sai
j£S&*
'Wt..^.' • -If*
Components
Propane
•>•.
$
.14.40
AvaContofCuttCA 270.5 pern
f-1. 00000
Constvui
IM 669000000
0*0.000000000
I , ,
t \ • f
IDftb
MTWI1688
A*A237840000
E*4LOOOQOOOOO
> V - ~
' •«»
'i*!. •
•Off
-------
Scott Specialty Gases, Inc.
6141 fcASTON ROAD. P.O. BOX310. PLUMSTEAUVlLLh. HA 1BSMSMU1U (IZlb) /tJb-«tibl—FAX, (2
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
Pacific Environmental Ser
C/O Virgin island Waters
Power Auth, 18 Sub Base
St Thomas, 000000
ANALYTICAL INFORMATION
Assay Laboratory
Scott Specialty Gases, inc.
6141 Easton Road
P.O. Box 310
Plumsteadville, PA 18949-0310
Purchase Order 10396-0115
Scott Project # 01-75518-007
This certification was performed according to EPA Traceabiliti/ Protocol For Assay & Certification of Gaseous Calibration Standards;
1 Procedure #G1, Section Number 3.0.4; September, 1993.
Cylinder Number ALM007003 Certification Date 01-30-% Expiration Date 01-30-99
Cylinder Pressure 2000 psig+ Previous Certification Dates None
ANALYZEDCYLINDER
Components
Propane
Balance Gas: Air
Certified Concentration
279 pom
Analytical Uncertainly*
±1%NIST Traceable
» Do not use when cylinder is less thin 150 psig.
'Analytical uncertainty a inclusive of usual known error sources which at least include! precision of the measurement pi'occuu.
REFERENCESTANDARD
Type Expiration Date
SRM1669
02-04-%
Cylinder Number
CLM000691
Concentration
464 ppm C3Ha in Nj
INSTRUMENTATION
Instrument/Model/Serial i
C3H8: Varian/VA3300/7945
Last Date Calibrated
01-04-%
Analytical Principle
FID
ANALYZER READINGS (Z-ZemGa* R-ReferenceGas T=TestGas r"Coti»Ution Coefficient)
Component*
Propane
First Triad Analysis
Second Triad Analysis
Calibration Curve
DatR 01-30-96 Resporne Units: Am
Zl-000000 Rl-471703 T1-2K318S
82-4714*7 Z2-000000 T2-29J234
Z3-000000 T3-2837M R3-472199
Avg. Cone of Out Cy 1279 ppm
r-1.00000
Comluitx
B-9J612E-03
OOOOOOE+OO
NTKM2646
C-O«XX)E+00
EK).OOOOE-K»
Special Notes:
**£* V: .
-------
Scott Specialty Gases, Inc.
6141 EASTON ROAD, P.O. 80X310, PLUMSTEADVILLE. PA 1894WB10
(215) 76M861 FAX (215) 76WJ320
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
Pacific Environmental Ser
C/O Virgin Island Waters
Power Auth, 18 Sub Base
St Thomas, 000000
ANALYTICAL INFORMATION
Assay Laboratory
Scott Specialty Gases, Inc
6141 Easton Road
P.O. Box 310
Plumsteadville, PA 18949-0310
Purchase Order 10396-0115
Scott Project # 01-75518-008
This certification was performed according to EPA Traceabilihf Protocol For Assay cV Certification of Caseous Calibration Standards;
1 Procedure ttGl, Section Number 3.0.4; September, 1993.
Cylinder Number ALM056112 Certification Date 01-30-% Expiration Date 01-30-99
Cylinder Pressure 2000psig-i- Previous Certification Dates None
1 ANALYZED CYLINDER
Components
Propane
Balance Gas: Air
Certified Concentration
451 ppm
Analytical Un
±1% MIST Traceable
+Do not uic when cylinder b leu than 150 piig. • '
'Anitybcal uncertainty b inclusive of usual known error sources which it le«»t includes precnion of the measurement processes.
REFERENCE STANDARD
Type Expiration Date
SRM1669 02-04-%
Cylinder Number
CLM000691
Concentration
464 ppm C3H« in Nj
INSTRUMENTATION
Instrument/Modd/Serial #
C3H& Varian/VA3300/7945
Last Date Calibrated
01-04-%
Analytical Principle
FID
ANALYZER READINGS (Z-ZeroGas R-Refetcnce Gas T°TcstGas r=Correlation Coefficient)
Components
Propane
Special Notes:
First Triad Analysis
Second Triad Analysis
Calibration Curve
Date 01-30-96 Response Unite: Arc*
Zl-000000 Rl-471709 Tl-458361
R2-471487 Z2-000000 T2-458222
Z3-000000 TJ-458621 R3-472199
Avg. Cone o( Cu»t Cyl 451 ppm
r-1.00000
Conamnts:
B-9J612E-03
D-O.OOOOE+00
hmCM2646
C-OJWOOE+00
E^»XMOOE+00
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STREET, TROY, Ml 48083
(810)589-2950 FAX:(810) 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENVIRONMENTAL SER
ATTN: GARY GUY
4700 DUKE DRIVE, STE 150
MASON, OH 45040
Assay Laboratory
Scott Specialty Gases. Inc
1290Comberinere
Troy, MI 48083
Purchase Order: 103-95-0238
Scott Project # : 578642
ANALYTICAL INFORMATION
This certification was performed according to EPA Traceabilicy Protocol For Assay and Certification ot Gaseous
Calibration Standards; Procedure G1; September. 1993.
Cylinder Number: AAL18513
.Cylinder Pressure + : 1900 psig
Certificate Date : 3/17/95 Expiration Date :
Previous Certificate Date : None
3/17/98
ANALYZED CYLINDER
Components
Propane
Certified Concentration
463 J ppm
Analytical Uncertainty*
±1% NIST Directly Traceable
Balance Gas: Air
+D6 not use when cylinder presume u below 150 psig.
•Analytical tccuncy ii inclusive of usual known error sources which it lean include precision of the measurement processes.
REFERENCE STANDARD
Type Expiration Date
.NJRM1668 677/96
Cylinder Number
ALM-032015
Concentration
95.5 ppm Propane in Air.
INSTRUMENTATION
Instrument/Model/Serial it
Prop:Beckman/400/1002059
Last Date Calibrated
222/95
Analytical Principle
Flame lonizalion Detection
..... ANALYZER READINGS (Z-Zero Gas R-Reference Gil T-Test Gas r-Correl«tion Coefficient)
;- . tr
Components
Propane
iK
m
First Triad Analysis Second Triad Analysis Calibration Curve
D**3M7/9S RMponMUnK mv
Z1-000 R1-14.40 -\>*».8O
R2«14.40 Z2^>.00 T24Q.60
Z»O.OO T3-M.SO R>14.40
A»»Cone.ofCu(tCyl 4S3.3ppm
r i«> k n •ri^Qt'tf *
r-i ooooo mmiieea
ConsurM: A*4UVMOOOO
B*4.fl68oooooo omnooffnioo
0*0.000000000 B^).000000000
&:<,-*&q^*?j4fc.
r^^^^^^^^^
' '
-------
1722 S. WENTWORTH AVENUE
IICAGO, IL 60628
Certificate of Analysis - EPA Protocol Gas Standard page i of i
IRFORMED ACCORDING TO EPA TRACEABILITY PROTOCOL FOR ASSAY AND CERTIFICATION OF GASEOUS CALIBRATION STANDARDS (PROCEDURE fGl)
Btomert Order No: CSS-363029-01
ROCHESTER - APCI Batch No: 861-30465
77 DEEP ROCK RD. Notes:
ROCHESTER NY 14624- Cylinder No: SG9168208BAL
• Cylinder Pressure*: 2000 psig
Certification Date: 02/05/96
pOt Rel: Expiration Date: 02/05/99
* Certified Concentration *** ********* Reference Standards ********* ************* Analytical Instrumentation *************
Certified Standard Instrument Serial Last Measurement
aponent Concentration Cylinder f Number Concentration Make/Model Number Calibration Principal
DPANB 464 ±2.9 PPM SG9126635BAL GMIS 503.6000 PPM Gow-Mac 750 59405U 01/16/96 GC-PID
Lance Gas: AIR
fgen Concentration 20.0 %
r* Standard should not be used below 150 psig
Approved By:
Richard VanDyke
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STREET, TROY, Ml 48083
(810)589-2950 FAX:(810) 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENVIRONMENTAL SER
ATTN: GARY GUY
4700 DUKE DRIVE. STE 150
MASON, OH 45040
Assay Laboratory
Scon Specialty Gases, Inc
I290Combennerc
Troy, MI 48083
Purchase Order: 103-95-0238
Scott Project # : 578642
ANALYTICAL INFORMATION
This certification was performed according to EPA Traceability Protocol For Assay and Certification of Gaseous
Calibration Standards; Procedure Gl; September, 1993.
.Cylinder Number: ALM028161 Certificate Date : 3/17/95 Expiration Date :
Cylinder Pressure •*•: 1900 psig Previous Certificate Date: None
3/17/98
ANALYZED CYLINDER
Components
Propane
Certified Concentration
886.7 ppm
Analytical Uncertainty*
±1% NIST Directly Traceable
Balance Gas: Air
+Oo KM use when cylinder pressure is below 150 psig.
*Aa»lyticil accuracy is incluavB 01 usual known error sources which «t least include precision of the measurement processes.
REFERENCE STANDARD
Expiration Date
6/7/96
trN
. I'.y'
•
Cylinder Number
ALM032015
Concentration .
95.5 ppm Propane in Air.
' INSTRUMENTATION
iBstrument/Model/Serial #
. Prop:Beckman/400/1002059
Last Date Calibrated
2/22/95
Analytical Principle
Flame lonization Detection
•*.'*•'
ANALYZER READINGS (Z-2*roGa§ It-Reference Gas T^TertGat r-Corrrianon Coefficient)
•^Components
Propane
First Triad Analysis
Second Triad Analysis
Calibration Carv» .
.;-SX&&®$.
-•iyi-r
(M«am/M RMponwUntt: mv
21-0.00 R1-1440 T1-1S3.00
R2>14.40 Z24LOO T2-133.00
Z>0.00 73^33.00 R>14.40
A»»Cene.o(CiaLCyL 688.7 ppm
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STREET, TROY, Ml 48083
CERTIFICATE OF ANALYSIS: EPA PROTOCOL
(810)589-2950 FAX:(810) 589-2134
Customer
PACIFIC ENVIRONMENTAL SER
4700 DUKE DRIVE, STE 150
MASON, OH 45040
Assay Laboratory
Scott Specialty Gases, Inc
l290Combcrmere
Troy, MI 48083
Purchase Order: 103-96-0206
Scott Project #: 96412
ANALYTICAL INFORMATION
]?>}*;certification was performed according to EPA Traceability Protocol For Assay and Certification of Gaseous
Calibration Standards; Procedure Ol; September, 1993.
! Cylinder Number: ALM005428
Cylinder Pressure + : 2000 psig
»£•. ANALYZED CYLINDER
Components
Propane
Certificate Date : 5/15/96 Expiration Date :
Previous Certificate Date : None
5/13/99
Certified Concentration
1737 ppm
Analytical Uncertainty*
±1% NIST Directly Traceable
Balance Gas: Air
' +Do not use when cylinder ptesuurc is below 150 psig.
•/..I .••.•Analytical accuracy is inclusive of usual known error jou
• <-" aa«^
irces which at least include precision of the measurement processes.
REFERENCE STANDARD
Expiration Date
677/96
.' •**;.'»,
"
INSTRUMENTATION
lutrument/Model/Serial #
C3tt8: Varian/1400/08982426
Cylinder Number
ALM032007
Last Date Calibrated
5/16/96
Concentration
95.3 ppm Propane in Air
Analytical Principle
Gas Chromatography
*..;. -,,,., .-ANALYZER READINGS (Z-ZeroCu R-RtftrenctGu T-TeitCu r-Correlation Coefficient)
. - ,:•'. Components First Triad Analysis Second Triad Analysis Calibration Curve
Date 6/1S/W RnporM Unto: my
Z1*O.OO R1*fi2S.OO 71408.80
R2-S25.00 Z24.00 12^86.80
ZM.OO T>«e7.10 R9*S2S.OO
A¥B.Conc.ofCu«.Cyl 1737 ppm
01.00000
NTW
8*1.707437000
0*0.000000000
../ ->v •&•
•'•***'***•*&'&..
Special Notn
• "^.'.^^fV-T- ;•'• :
Iti^, J»" -4l^»
-------
Scott Specialty Gases, Inc.
1290 COMBERMERE STREET, TROY, Ml 48083
(810)589-2950 FAX:(810) 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENVIRONMENTAL SER
ATTN: GARY GUY
4700 DUKE DRIVE, STE 150
MASON, OH 45040
Assay Laboratory
Scott Specialty Gases, inc
1290Combermere
Troy, MI 48083
Purchase Order: 103-97-0143
Scott Project #: 510863
ANALYTICAL INFORMATION
This certification was performed according to EPA Traceability Protocol For Assay and Certification of Gaseous
Calibration Standards; Procedure Gl; September, 1993.
Cylinder Number: ALM066778
Cylinder Pressure + : 1900psig
Certificate Date: 4/28/97
Previous Certificate Date : None
Expiration Date: 4/28/2000
ANALYZED CYLINDER
Components
Propane
Certified Concentration
2418 ppm
Analytical Uncertainty*
±1% NIST Directly Traceable
Balance Gas: Air
+Do not UK when cylinder preusun n below 150 pa g.
' Amlyncil iccuracy ii inclusive of uiuil known error ioureei which ii lent include precision of ihe measurement processes.
REFERENCE STANDARD
Type Expiration Date
NTRM2646 6/12/98
Cylinder Number •
AAL18338
Concentration
973 ppm Propane in Nitrogen
INSTRUMENTATION
Instrument/Model/Serial #
C3H8: Varian/1400/08982426
Last Date Calibrated
4/28/97
Analytical Principle
Gas Chromotography
ANALYZER READINGS (Z-ZcroGw R-ReferenceGM T-TcitGns r-Correladon Coefficient)
.•*;
Components
Propane
' ' 't.
•^
First Triad Analysis Second Triad Analysis
DMK4/20/B7 Rxpnrm Unte mv
Z1«0.00 RK.415.00
TI-5,997.00
R2rt.415.00 Z2-O.OO T2-S.974.00
ZWJOO T3-6.994.00
Kfe^cllfePflr Cmt Cyi 241 B ppm
Calibration Curve
_ . A-n--/»1'ift^t»1*
p>1. 00000 NTRM2B46
CamUftK A"-J.J07WOOOO
B-0.4O42B8300 OaOOOOOOOOO
0^)000000000 E-0.000000000
Special Notes
•
-------
Scott Specialty Gases, Inc.
I4H) OJMBbKMbHh SIHbbl. TROY. Ml 48083 (810) 589-2950 FAX:<810) 589-2134
CERTIFICATE OF ANALYSIS: EPA PROTOCOL GAS
Customer
PACIFIC ENV1ROMENTAL SER
4700 DUKE DRIVE
STE150
MASON, OH 45040
Assay Laboratory
Scott Specialty Gases, Inc
l290Combcnnere
Troy, MI 48083
Purchase Order: 103-94-0070
Scott Project #: 56864
ANALYTICAL INFORMATION
This certification was pertbnned according to EPA Traceability Protocol For Assay and Certification of Gaseous
Calibration Standards; Procedure Gl; September. 1993.
Cylinder Number : AAL3345
Cylinder Pressure + : 1900 psig
Certificate Date : 7/22/94 Expiration Date :
Previous Certificate Date : None
7/22/97
ANALYZED rVT.INTtFR
Components
Propane
Certified Concentration
4507 ppm
Analytical Uncertainty*
±1% NIST Directly Traceable
Balance Gas: Nitrogen
+Do not use when cylinder pressure is below 150 piig.
'Anilyticil tccuracy ii inclusive of uiuii known error sources which n lean include precision of the roeaiuremaii processes.
Rg.FF.RENCF. STANDARD
Type
.OMIS
Expiration Date
1/2/96
Cylinder Number
ALM-030280
Concentration
4981 ppm Propane in Air
... INSTRUMENTATION
Instrument/Model/Serial #
Propane: Beckman/400/1002059
Last Date Calibrated
6/30/94
Analytical Principle
Flame ionization Detector
ANALYZER READINGS (Z-ZtroGu R-RefcrenceGas T-TestGai r-CorrtUfJoo Cotffldent)
Components
Propane
j&iA
m
®?i? "••
First Triad Analysis Second Triad Analysis Calibration
Z1-0.00 R1HOO.OO ri.go.eo
R2>100.00 224.00 T7*M.60
23*0.00 TO40.60 R3>100lOO
A*g.Conae«Cu»».CA 4507 ppm
CoftCMMVMiMM
M. 00000
CanMrtK
B-4aii2oaooa
0*0.000000000
mMiHL8inas,it • '
Curve
I C*Oj09MWOO
•VSj' ' •' :
.•WOsft;
• v-is-if^ '
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APPENDIX E
PROJECT PARTICIPANTS
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PROJECT PARTICIPANTS
EPA/EMC
Solomon Ricks
Kathy Weant
EPA/ESP
Madeleine L. Strum, PhD
Lasco Panel Products
Hilary North
Bruce L. Westbrook
Lasco Consultant
Robert Haberlein
Composites Institute
John Schweitzer
PES Air Sampling
John Chehaske
Frank Meadows
Dan Scheffel
Ron Kolde
Paul Siegel
Troy Abemathy
Gary Gay
PESOA
Wayne Westbrook
Kentucky Division of Air Quality
John Allen
PES Process
Kenneth Meardon, PhD
Melanie Proctor
Andrew Weisman
Deeco Air Sampling
Bill DeWees
Marc Hamilton
Brian Palm
Deeco Method 18 Analytical
Pete Zimmick
Barry Rayfield
Atlantic Technical Services -Air Sampling
Dave Savia
Enthalpy Analytical. Inc.
Todd Grosshandler
Bruce Rhodes
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TECHNICAL REPORT DATA
Please read instructions on the reverse before completing
1. REPORT NO.
EPA-454/R-99-024c
2.
4. TITLE AND SUBTITLE
Air Emissions From Reinforced Plastics Manufacturing Process, LASCO Panel
Products: Volume III * .
Ccvnoe?) T^-
Volume III of III
7. AUTHOR(S)
Franklin Meadows
Daniel F. Scheffel
9. PERFORMING ORGANIZATION NAME AND ADDRESS
Pacific Environmental Services, Inc.
Post Office Box 12077
Research Triangle Park, North Carolina 27709-2077
12. SPONSORING AGENCY NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Emissions, Monitoring and Analysis Division
Research Triangle Park, North Carolina 277 1 1
3. RECIPIENT'S ACCESSION NO.
5. REPORT DATE
August 1999
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO.
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-D-70069
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
15. SUPPLEMENTARY NOTES
16. ABSTRACT
The United States Environmental Protect
and Analysis Division (EMAD), Emission M
manufacturing source category to properly se
Amendments of 1 990. The reinforced plastic
by the ESD as the host facility for this emissi
The sampling program was designed to
by reinforced plastic manufacturing, 2) Ident
area, 3) Evaluate three ventilation scenarios,
emission limitation achieved by the use of a \
emissions from a continuous lamination proc
options involving emissions abatement, and (
of raw material and the addition of a gel coat
Sampling was performed during 13 proc
and methyl methacrylate (MMA), and the ai
emissions of HAPs from the oven stacks.
This volume (Volume III) is comprised c
(Project Participants).
ion Agency (EPA) Emission Standards Division (ESD) requested that the EPA's Emissions Monitoring
sasurement Center (EMC) provide testing support in the investigation of the reinforced plastics composite
t the Maximum Achievable Control Technology (MACT) standards as required by the Clean Air Act
s composite manufacturing process located at LASCO Panel Products in Florence, Kentucky was selected
ons testing program.
support the following ESD objectives: 1) Identify and quantify the hazardous air pollutants (HAPs) emitted
fy the sources of HAPs and the total HAPs mass emission rates from the wet application area and the oven
4) Depending on the effectiveness of the industry proposed "closed" system, develope a performance-based
vet area enclosed table system, 5) Assess the existing emission factors for volatile organic compound
ess for the purposes of updating the information in AP-42 and determining cost effectiveness for MACT
i) Determine the effect of various process paramenters such as line speed, laminate thickness, HAP content
layer on the emission factor.
sss operating conditions. Measurements were made of the total hydrocarbons (THC), styrene, cumene,
r flow rate at all enclosure exhausts. A secondary objective of the sampling program was to obtain the
>f 799 pages and consists of Appendices B (Analytical Data), C (Calculations), D (QA/QC Data), and E
17. KEY WORDS AND DOCUMENT ANALYSIS
a. DESCRIPTIONS
Cumene
Emission Measurements
Hazardous Air Pollutants
Lamination Process
Methyl Methacrylate
Reinforced Plastics Manufacturing
Styrene
Total Hydrocarbons
Volatile Organic Compounds
18. DISTRIBUTION STATEMENT
Unlimited
b. IDENTIFIERS/OPEN ENDED TERMS
1 9. SECURITY CLASS (This Report)
Unclassified
20. SECURITY CLASS (This page)
Unclassified
c. COASTI Field/Group
21. NO. OF PAGES
4&fr ~?<^
22. PRICE
EPA Form 2220-1 (Rev. 4-77) PREVIOUS EDITION IS OBSOLETE
F:\U\FMeadows\TRD.Frm\WP 6.1
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