United States
Environmental Protection
Agency
Office of
Pollution Prevention and Toxics
7404
EPA747-R-94-001
July. 1994
SEMI VOLATILE ORGANIC
COMPOUNDS IN THE
GENERAL U.S. POPULATION
NHATS FY86 RESULTS
VOLUME II: Appendices
-------
SBMIVOLATILE ORGANIC COMPOUNDS IN THE GENERAL U.S. POPULATION I
NHATS FY86 RESULTS
VOLUME Hi APPENDICES
This work was supported by the
U.S. Environmental Protection Agency
under EPA contract numbers 68-02-4294, 68-D8-0115,
68-DO-0126, 68-D2-0139, 68-02-4252, 68-02-4293,
and 68-D9-0174
Prepared for
Khoan Dinh, Work Assignment Manager
Technical Programs Branch
Chemical Management Division
Office of Pollution Prevention and Toxics
U.S. Environmental Protection Agency
Washington, DC 20460
July 1994
R*eyol«d/R«cyotabl«
Prtnwd with 8oy/C«no(« Ink on paper tlun
contain* at IMMI 60% rwycM fiber
-------
TABLE OF CONTESTS
Volume II
Appendix A:
Appendix B:
Appendix C:
Appendix D:
Appendix c.:
Appendix F:
Appendix G:
Appendix H:
Appendix I:
Appendix J:
Listing of NHATS FY86 Composite Data
Listing of NHATS FY86 QC Data For Corpounds
Detected in At Least 50% of Composites (plus
Octachlorobiphenyl)
Plots of Observed vs. Spiked Concentrations for
Spiked Semivolatile Compounds Detected in At Least
50% of Composites (plus Cotachlorobiphenyl) .
Plots of Observed Concentration vs. Batch ID
for Unspiked Semivolatiie Co-pounds Detected ir.
At Least 50% of Cc-posites
Sunnary of QC Data for the FY56 NHATS Spiked
Semivolatile Compounds Not or. the Target list fcr
Statistical Analysis
Characterizing the Distribution of NHATS FY86
Semi volatile Compound Concentrations (ir. r.g/g.
Unadjusted for Surrogate Recoveries) Based or. Ai_
50 Composite Samples
Estimates of Average Concentrations with 55%
Confidence Intervals As Determined by the Additive
Model, for Selected Subpcpulations ir. the FYS5
NHATS
Concentrations (ng/g) fro- the FY82, FY84, and FY5-
NHATS, Plotted in Chronological Order with Age
Group as the Plotting Symbol
Surrogate-Adjusted Concentrations (ng/g) fro- the
FY82, FY84, and FY86 NHATS, Plotted in
Chronological Order vith Age Group as the Plotting
Symbol
Arithmetic Averages (and Standard Errors) of
Extractable Lipid Concentrations (ng/g) for
Compounds Analyzed in the FY86 NHATS and Also
Analyzed in the FY82 and/or FY84 NHATS
Comparisons of Predicted Average Concentrations
(n9/9) by Selected Subpopulations for Selected
Semivolatiles over the FY82, FY84, and FY86 NHATS
-------
TABLE OP CONTENTS (cont.)
Volume II (cont.)
Appendix K: Plots of Estimates Average Concentrations (ng/g) by
Census Region and by Age Group, Plus and Minus Two
Standard Errors, Based on the Additive Model for
the FY82, FY84, and FY86 NHATS
-------
APPENDIX A
Listing of NHATS FY86 Composite Data
-------
Semivolatile organic compounds included in the following listing
of lipid-adjusted concentrations are denoted by ID numbers. The
ID numbers and their corresponding compound names are as follows:
Compound # Compound Name
PESTICIDES
1 P,P-DDT
2 O,P-DDT
3 P,P-DDE (M/Z=288)
4 O,P-DDE
5 O,P-DDD
6 ALPHA-BHC
7 BETA-BHC
8 DELTA-BHC
9 GAMMA-BHC(LINDANE)
10 ALDRIN
11 HEPTACHLOR
12 HEPTACHLOR EPOXIDE
13 OXYCHLORDANE
14 TRANS-NONACHLOR
15 GAMMA-CHLORDANE
16 MIREX
60 DIELDRIN
61 ENDRIN
62 ENDRIN KETONE
300 P,P-DDE (M/Z=316)
600 DIELDRIN (CORRECTED)
CHLOROBENZENES
17 1,3-DICHLOROBENZENE
18 1,4-DICHLOROBENZENE
19 1,2-DICHLOROBENZENE
20 1,2,3-TRICHLOROBENZENE
21 1,2,4-TRICHLOROBENZENE
22 1,3,5-TRICHLOROBENZENE
23 1,2,3,4-TETRACHLOROBENZENE
24 1,2,3,5-TETRACHLOROBENZENE
25 1,2,4,5-TETRACHLOROBENZENE
26 PENTACHLOROBENZENE
27 HEXACHLOROBENZENE
PAHS
41 NAPHTHALENE
42 ACENAPHTHALENE
A-l
-------
Compound IDs and their corresponding compound names:
Compound # Compound Name
PAHs (cont.)
43 ACENAPHTHENE
44 FLUORENE
45 PHENANTHRENE
46 FLUORANTHENE
47 PYRENE
48 CHRYSENE
49 BENZO (A) PYRENE
PCBs
50 MONOCHLOROBIPHENYL
51 DICHLOROBIPHENYL
52 TRICHLOROBIPHENYL
53 TETRACHLOROBIPHENYL
5 4 PENTACHLOROBIPHENYL
55 HEXACHLOROBIPHENYL
56 HEPTACHLOROBIPHENYL
57 OCTACHLOROBIPHENYL
5 8 NONACHLOROBIPHENYL
59 DECACHLOROBIPHENYL
PHTHALATE ESTERS
63 DIMETHYL PHTHALATE
64 DIETHYL PHTHALATE
65 DI-N-BUTYL PHTHALATE
66 BUTYL BENZYL PHTHALATE
67 BIS (2-ETHYLHEXYL) PHTHALATE
PHOSPHATE TRIESTERS
68 TRIBUTYL PHOSPHATE
69 TRIS (2-CHLOROETHYL) PHOSPHATE
70 TRIS (2,3-DIBROMOPROPYL) PHOSPHATE
71 TRIPHENYL PHOSPHATE
72 TRITOLYL PHOSPHATE
OTHER (quantitative)
28 BIPHENYL
29 l,2-DIBROMO-3-CHLORO PROPANE
30 HEXACHLORO BUTADIENE
A-2
-------
Compound IDs and their corresponding compound names:
Compound #
Compound Name
OTHER (quantitative) (cont.)
31 HEXACHLORO CYCLOPENTADIENE
32 2,2',4',5-TETRABROMO BIPHENYL
33 0-CYMENE
34 D-LIMONENE
35 D,L-ISOBORNEOL
36 1-INDANONE
37 2-INDANONE
38 BUTYLATED HYDROXYTOLUENE
39 COUMARIN
40 OCTAMETHYL-CYCLOTETRASILOXANE
73 ETHYL HYDROCINNAMATE
74 2-METHOXY-3-METHYLPYRAZINE
75 2,2',4,4',5-PENTACHLORO DIPHENYL ETHER
76 4-CHLORO-P-TERPHENYL
77 TRICHLORO-P-TERPHENYL
78 2-PHENYL PHENOL
PESTICIDES (qualitative)
85 ISOPHORONE
86 DICHLOROVOS
98 CHLORPYRIFOS
99 ISOPRQPALIN
100 BUTACHLOR
101 NITROFEN
102 PERTHANE
106 DICOFOL
107 P.P'-METHOXYCHLOR
CHLORINATED AROHATICS (qualitative)
88
89
90
91
92
95
96
97
110
2,4,6-TRICHLOROANISOLE
2,4,6-TRICHLOROPHENOL
2,4,5-TRICHLOROPHENOL
2,3,6-TRICHLOROANISOLE
2,3,6-TRICHLOROPHENOL
PENTACHLOROANISOLE
PENTACHLORONITROBENZENE
2,3,4-TRICHLOROANISOLE
OCTACHLORONAPHTHALENE
A-3
-------
Compound IDs and their corresponding compound names;
Compound # Compound Name
PAHs (qualitative)
105 BENZO (A) ANTHRACENE
108 BENZO (B) FLUORANTHENE
109 BENZO (K) FLUORANTHENE
111 DIBENZO (A,H) ANTHRACENE
OTHER (qualitative)
79 1-NONENE
80 CUMENE
81 1,2,4-TRIMETHYLBENZENE
82 HEXYL ACETATE
83 1,3-DIETHYLBENZENE
84 1,4-DIETHYLBENZENE
87 QUINOLINE
93 DIBENZOFURAN
94 CHLORDANE
103 CHLOROBENZYLATE
104 BIS (2-ETHYLHEXYL) ADIPATE
A-4
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 HEATS (Unadjusted for Surrogate Recoveries)
Group = Pesticides
>
Compound # (see page A-l)
Lab #/Samp. #/Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS8600289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
1
90.2
138
88
64.4
457
30.6
21.3
6.2°
40.9
114
129
244
562
1470
42.1
160
113
572
161
715
427
109
252
48.1
167
143
707
173
65.5
135
501
2
5.75°
5.95°
6.85°
6.15°
6.9°
7.7°
7.7°
6.55°
7.7"
6.85°
5.75n
6.95*
5.95°
6.95°
16.2°
6.8°
6.5°
5.65°
7.7°
6.65n
3.27"
3.185"
2.725n
5.8"
2.81"
3.895°
3.46°
35.75°
3.08°
2.94°'
3.1°
3
1490
1470
963
1090
4180
617
2690
2270
291
2500
2280
3000
2530
1680
710
2060
1640
7140
887
3030
1820
1350
1040
1140
2320
1580
3060
545
796
4460
11100
4
7.2°
7.5°
8.65°
7.7°
8.65°
9.7°
9.7°
8.25°
9.7°
8.6°
7.25°
8.75°
7.45°
8.75°
20.4°
8.55°
8.15°
7.15°
9.7°
8.35°
4.12°
4.01°
3.43°
7.3°
3.54°
4.91°
4.355°
45°
3.88°
3.7°
3.905°
5
7.1°
7.4°
8.5°
7.6°
8.5°
9.5°
9.5°
8.1°
9.55°
8.45°
7.15°
8.6°
7.35°
8.6°
20°
8.4°
8.05°
7°
9.55°
8.2°
4.045°
3.94°
3.37°
7.15°
3.48°
4.82°
4.28°
44.2°
3.81°
3.635°
3.835°
6
5.8°
6°
6.9°
6.2°
6.95°
7.75°
7.75°
6.6°
7.8°
6.9°
5.8°
7°
6°
7°
16.3°
6.85°
6.55°
5.7°
7.8°
6.7°
3.3°
3.21°
2.745°
5.85°
2.835°
3.93°
3.49°
36.05°
3.105°
2.965°
3.13°
7
154
146
61
32.5
326
20. 11
161
403
49.7
284
234
237
250
7.6°
17.7°
474
93.7
308
354
266
514
114
285
66.7
462
319
344
39.1°
53.8
192
349
8
6.45°
6.75°
7.75°
6.9°
7.75°
8.65°
8.65°
7.35°
8.7°
7.7°
6.5°
7.8°
6.7°
7.85°
18.25°
7.65°
7.3°
6.4°
8.7°
7.5°
3.685"
3.59°
3.07°
6.5°
3.17°
4.395°
3.9°
40.3°
3.47°
3.315°
3.495°
9
118
6.45°
7.4°
6.65°
7.45°
8.3°
8.3°
7.1°
38.84
7.4°
6.25°
7.5°
6.4°
7.55°
17.5°
7.35°
7°
6.1°
8.35°
7.15°
3.54°
3.445°
2.945°
6.25°
3.04°
4.215°
3.74°
38.65°
3.33°
3.18°
3.355°
10
9.3°
6.25°
7.2°
6.4°
7.2°
8.05°
8.05°
6.85°
8.1°
7.15°
6.15°
7.3°
6.2°
7.3°
16.95°
7.15°
6.8°
5.95°
8.1°
6.95°
3.43"
3.34"
2.855°
6.05°
2.95°
4.085°
3.625°
37.5°
3.23°
3.08°
3.25°
11
12.55°
6°
6.9°
6.15°
6.95°
7.75°
600°
6.6°
7.75°
6.9°
8.95°
10.3*
5.95°
7°
16.3°
6.85°
6.55°
5.7°
7.75°
6.7°
3.295°
3 . 205°
2.74°
5.8°
2.83°
3.925°
3.48°
36°
3.1°
2.96°
3.12°
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Pesticides (cont.)
>
a\
Compound # (see page A-l)
Lab #/Samp. #/Batch
17947 ACS8600500
17948 ACS8600350
17949 ACS8600216
17951 ACS8600261
17953 ACS8600305
17955 ACS8600145
17956 ACS8600118
17958 ACS8600341
17959 ACS8600127
17960 ACS8600181
17962 ACS8600083
17965 ACS8600332
17967 ACS8600109
17968 ACS8600207
17969 ACS8600047
17970 ACS8600234
17986 ACS8600314
17987 ACS8600056
17988 ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
1
13.2
114
588
75.5
2.94°
8.07
7.19
562
306
164
156
240
117
437
130
124
128
64.6
172
2
3.07°
3.15°
3.165°
3.88°
3.775°
3.315°
2.7805°
3.02°
3.005°
3.125°
2.85°
3.11°
2.945°
3.205°
2.905°
2.975°
3.295°
2.93°
3.105°
3
2290
3660
7110
1110
442
2210
4880
11400
5410
3790
3450
8340
2960
7330
2050
2300
6320
1150
2630
4
3.87°
3.965°
3.985°
4.885°
4.755°
4.175°
3.502°
3.8°
3.78°
3.935°
3.59°
3.915°
3.71"
4.035°
3.66°
3.75°
4.15°
3.69°
3.915°
5
3.8°
3.895°
3.915°
4.8°
4.67°
4.105°
3.44°
3.735°
3.715°
3.915°
3.53°
3.845°
3.645°
3.965°
3.595°
3.68°
4.075°
3.625°
3.845°
6
3.1°
3.175°
3.19°
3.91°
3.81°
3.345°
2.805°
3.045°
3.03°
3.155°
2.875°
3.135°
2.97°
3.235°
2.93°
3°
3.325°
2.955°
3.135°
7
224
181
581
207
4.13°
45.1
233
296
279
150
155
418
188
256
101
105
107
206
118
8
3.46°
3.55°
3.565°
4.37°
4.255°
3.74°
3.1345°
3.4°
3.385°
3.525°
3.215°
3.505°
3.32°
3.615°
3.275°
3.355°
3.715°
3.305°
3.505°
9
3.32°
3.405°
3.42°
4.195°
4.085°
3.585°
3.0075°
3.265°
3.25°
3.38°
3.085°
3.365°
3.185°
3.465°
3.14°
3.22°
3.565°
3.17°
3.36°
10
3.22°
3.3°
3.315°
4.065°
3.96°
3.48°
2.9155°
3.165°
3.15°
3.28°
2.99°
3.26°
3.09°
3.36°
3.045°
3.12°
3.455°
3.075°
3.26°
11
3.09°
3.17°
3.185°
3.905°
3.8°
3.34°
2.7995°
3.04°
3.025°
3.145°
2.87°
3.13°
2.965°
3.225°
2.925°
2.995°
3.315°
2.95°
3.13°
Not detected; concentration represented by one-half the detection limit.
reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Oroup = Pesticides (cont.)
Compound # (see
Lab #/Samp. if/Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS86Q0289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
12
46.7
44.9
45.5
28.6
122
41.6
84.3
111
7.35"
45.8
125
82.9
106
6.6"
66.4
118
93.8
93.7
26.5
172
102
54.7
84.3
50.3
194
51.1
82.3
33.95°
25.2
119
218
13
6.65"
352
7.95°
7.1n
7.95n
8.9n
133
7.55"
8.9n
7.9°
168
183
159
223
42.6
182
143
209
84.5
212
168
95.9
183
46.7'
140
4.505n
181
41.35"
38.6
190
366
14
163
92
49.3
5.95"
54.5
7.45°
218'
37
60.2
136
5.6"
444
238
117
62.1
219
163
362
49
322
206
95.1
18
79.1
159
89
203
34.75"
48.8
207
612
15
5.7"
5.9"
6.8"
6.05"
6.8"
7.6"
7.6"
6.5"
7.65"
6.75"
5.7"
6.9°
5.9"
6.9"
16.05°
6.75°
6.45°
5.6°
7.65"
6.55°
3.24°
3.155"
2.7°
5.75"
2.785"
3.865"
3.43°
35.45°
3.05"
2.915"
3.075"
16
22.6
5.8°
6.65°
5.95"
51.6
7.45"
7.45"
6.35n
7.5°
33.5
24.4
28.2
23.7
6.75°
15.75°
16.4
19
5.5"
7.5"
29
31.1
14.8
17.4
5.6"
2.735"
3.79"
3.365"
34.75°
2.995"
2.86"
22.4
60
27"
28.05°
32.25°
28.8"
96.8
36.15°
36.15°
30.8°
36.3"
32.15"
54.5°
94.1
114
32.75"
76°
74.2
255
53"
72.5"
62.5"
92.5"
29.95°
77°
54.5°
26.45"
36.7°
65°
336.5"
28.95"
83"
87.5"
page A-l)
61
33.45"
34.8"
39.95"
35.7°
40.1°
44.8°
44.8"
38.15°
45°
39.8°
67.5"
40.45"
34.6"
40.55"
94.5"
39.65"
37.85°
66"
90"
77.5°
114.5"
37.1"
95.5°
67.5"
32.8"
45.45"
80.5"
417°
35.9°
103"
108.5"
62
19.6"
20.35°
23.4"
20.9"
23.5"
26.25"
26.25"
22.35"
66. 7l
23.3"
39.4°
23.7"
20.25"
23.75"
55°
23.2°
22.15°
38.65°
52.5°
45.3"
67"
21.75"
56"
39.5"
19.2"
26.6"
47.25"
244"
21"
60°
63.5"
300
1370
1460
1530
1030
2650
564
2570
2240
273
2310
2120
2750
1660
1600
673
1920
1510
6690
878
2380
943
1200
538
1130
1130
1550
2000
534
785
4730
12900
600
27"
48.9
43.7
33.6
96.8
36.15"
36.15"
30.8"
36.3"
47.3
54.5°
94.1
114
32.75°
76"
74.2
255
53"
72.5"
62.5"
92.5°
12l
77"
7.77'
37.7
36.7°
9.21
336.5"
20'
25.4
40.6
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 MEATS (Unadjusted for Surrogate Recoveries)
Group = Pesticides (cont.)
>
00
Compound t (see
Lab //Samp. //Batch
17947 ACS8600500
17948 ACS8600350
17949 ACS8600216
17951 ACS8600261
17953 ACS8600305
17955 ACS8600145
17956 ACS8600118
17958 ACS8600341
17959 ACS8600127
17960 ACS8600181
17962 ACS8600083
17965 ACS8600332
17967 ACS8600109
17968 ACS8600207
17969 ACS8600047
17970 ACS8600234
17986 ACS8600314
17987 ACS8600056
17988 ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
12
77.4
64.4
83.8
37.3
11.5
103
173
66.2
131
95.6
140
71.5
80.7
119
73
49.5
45.7
79.7
81.1
13
108
142
96.1
4.485°
152
186
202
140
216
157
160
180
118
175
92.3
108
63.9
94.8
140
14
173
143
172
75.3
57.2
227
269
218
256
325
256
239
122
350
114
147
72
88.4
167
15
3.04°
3.12°
3.135°
3.845°
3.745°
3.29°
2.7565°
2.99°
2.975°
3.1°
2.825°
3.08°
2.92°
3.175°
2.88°
2.95°
3.265°
2.905°
3.08°
16
40.7
3.065°
3.075°
3.775°
3.675°
31.4
2.705°
2.935°
2.92°
3.04°
2.775°
3.025°
2.865°
9.7'
2.825°
2.895°
3.205°
2.85°
3.025°
60
28.9°
59.5°
89.5°
157
35.55°
62.5°
78.5°
85°
85°
29.4°
80.5°
58.5°
55.5°
90.5°
54.5°
84°
62°
55°
58.5°
page A-l)
61
35.8°
73.5°
110.5°
90.5°
44°
77.5°
97.5°
105.5°
105°
36.45°
100°
72.5°
68.5°
112°
67.5°
104°
77°
68.5°
72.5°
62
20.95°
43°
65°
53°
25.8°
45.3°
57°
62°
61.5°
21.35°
58.5°
42.45°
40.2°
65.5°
39.65°
61°
45°
40.05°
42.45°
300
2070
3460
7240
1000
382
2020
4570
14300
6390
3790
3260
8890
2980
7600
2010
2240
6190
1080
2560
600
47.9
27.8'
21.1
157
35.55°
7.91'
78.5°
7.411
22.3'
29.4°
37.3
58.5°
35.9
24.6*
35.7
9.671
8.58'
21. 11
30.2
* Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 MEATS (Unadjusted for Surrogate Recoveries)
Group = Chlorobenzenes
Compound t ( see
Lab #/Samp. //Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS8600289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
17
5.35°
5.5*
6.35°
5.65°
6.35°
7.1°
7.1°
6.05°
7.15°
6.3°
5.35°
6.4"
5.5°
6.45°
14.95°
6.3°
6°
5.25°
7.15°
6.15°
3.025°
2.94°
2.515°
5.35°
2.6°
3.6°
3.195°
33.05°
2 . 845°
2.715°
2.865°
18
52.2
32.3
5.7°
120
240
43.7
245
5.45°
6.45°
113
25.7
165
195
5.8°
152
68.2
125
12.6
92.1
77.3
115
14.2
102
32.6
48
220
34.4
29.85°
2.57°
8.18
85.3
19
5.3°
5.5°
6.35°
5.65°
6.35°
7.1°
7.1°
6.05"
7.15°
6.3°
5.35°
6.4°
5.5°
6.45°
14.95°
6.3°
6°
5.25°
7.15°
6.15°
3.025°
2.945°
2.52°
5.35°
2.6°
3.605°
3.2°
33.05°
2.85°
2.72°
2.87°
20
6.2°
6.45°
7.4°
6.6°
7.4°
8.3°
8.3°
7.05°
8.3°
7.35°
6.2°
7.5°
6.4°
7.5°
17.45°
7.35°
7°
6.1°
8.3°
7.15°
3.525°
3.43°
2.935°
6.25°
3.03°
4.2°
3.73°
38.5°
3.32°
3.17°
3.34°
21
5.35°
5.55°
6.4°
5.7°
6.4"
7.15°
7.15°
6.1°
7.2°
6.35°
5.35°
6.45°
5.5°
6.5°
15.05°
6.35°
6.05°
5.25°
7.2°
6.15°
3.045°
2.965°
2.535°
5.4°
2.62°
3.63°
3.22°
33.3°
2.865°
2.735°
2.885°
22
5.8°
6.05°
6.95°
6.2°
7°
7.8°
7.8°
6.65°
7.85°
6.95°
5.85°
7.05°
6°
7.05°
16.4°
6.9°
6.6°
5.75°
7.8°
6.75°
3.32°
3.23°
2.76"
5.85°
2.855°
3.955°
3.51°
36.25°
3.125°
2.98°
3.145°
page A-l)
23
6.15°
6.4°
7.35°
6.55°
7.35°
8.25°
8.25°
7°
8.25°
7.3°
6.2°
7.45°
6.35°
7.45°
17.35°
7.3°
6.95°
6.05°
8.25°
7.1n
3.505°
3.41°
2.92°
6.2°
3.015°
4.18°
3.71°
38.3°
3.3°
3.15°
3.325°
24
6.1°
6.35°
7.3°
6.5°
7.3°
8.15°
8.15°
6.95°
8.2°
7.25°
6.15°
7.35°
6.3°
7.4°
17.2°
7.2°
6.9°
6°
8.2°
7.05°
3.475°
3.38°
2.89°
6.15°
2.985°
4.14°
3.675°
37.95°
3.27°
3.12°
3.295°
25
5.65°
5.9"
6.75°
6.05°
6.8°
7.6°
7.6°
6.45°
7.6°
6.75°
5.7°
6.85°
5.85°
6.85°
15.95°
6.7°
6.4°
5.6°
7.6°
6.55°
3.23°
3.145°
2.69°
5.7°
2.775°
3.85°
3.415°
35.3°
3.04°
2.905°
3.06°
26
5.3°
5.5°
6.35°
5.65"
6.35°
7.1°
7.1"
6.05°
7.15°
6.3"
5.35°
6.4°
5.5°
6.45"
14.95°
6.3°
6°
5.25°
7.15°
6.15°
3.025°
2.94°
2.515°
5.35°
2.6°
3.6°
3.195°
33.05°
2 . 845°
2.715°
2.865°
27
36
54.2
24.8
15.9
76
15.9'
36.7
50.7
17.9*
32.8
43.9
53.2
31.6
44.8
35.9
62.2
43.7
92.8
20.3
77.3
58
34.5
47.3
38.9
47.6
29.5
96.3
34.1°
15
50.7
68.4
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the PY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Chlorobenzenes (cont.)
Compound f (see
Lab #/Samp. #/Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
17
2.84°
2.91°
2.925°
3.585n
3.49°
3.065n
2.57°
2.79°
2.775°
2.89°
2.635°
2.875°
2.72°
2.96°
2.685°
2.75°
3.045°
2.71°
2.87°
18
28
54.6
279
14
29.5
60
87.5
10.9
52.5
30.1
247
174
33.1
28.5
150
2.485°
12.6
35.3
114
19
2.84°
2.915°
2.925°
8.2"
3.495°
3.07°
2.5725°
2.79°
2.78°
2.89°
2.64°
2.875°
2.725°
2.965°
2.685°
2.755°
3.05°
2.71°
2.875°
20
3.31°
3.395°
3.41°
4.18°
4.07°
3.575°
2.997°
3.255°
3.235°
3.37n
3.075°
3.35°
3.175°
3.455°
3.13°
3.205°
3.55°
3.16°
3.35°
21
2.86°
2.93°
2.945°
3.61°
3.515°
3.09°
2.5885°
2.81°
2.795°
2.91°
2.655°
2.895°
2.74°
2.985°
2.705°
2.77°
3.065°
2.73°
2.895°
22
3.115°
3.195°
3.205°
3.935°
3.83°
3.365°
2.821°
3.06°
3.045°
3.17°
2.895°
3.155°
2.985°
3.25°
2.945°
3.02°
3.345°
2.975°
3.155°
page A-l)
23
3.29°
3.375°
3.39°
4.16°
4.045°
3.555°
2.9805°
3.235°
3.22°
3.35°
3.055°
3.33°
3.155°
3.435°
3.115°
3.19°
3.53°
3.14°
3.33°
24
3.26°
3.345°
3.36°
4.12°
4.01°
3.525°
2.9535°
3.205°
3.19°
3.32°
3.03°
3.3°
3.13°
3.405°
3.085°
3.16°
3.5°
3.115°
3.3°
25
3.03°
3.11°
3.125°
3.83°
3.73°
3.275°
2.7455°
2.98°
2.965°
3.085°
2.815°
3.07°
2.905°
3.165°
2.87°
2.94°
3.255°
2.895°
3.07°
26
2.84°
2.91°
2.925°
3.585°
3.49°
3.065°
2.57°
2.79°
2.775°
2.99°
2.635°
2.875°
2.72°
2.96°
2.685°
2.75°
3.045°
2.71°
2.87°
27
34.9
199
69.6
36.4
35.2
33.3
70.7
84.6
74.7
45.2
52.7
96.5
53.7
183
40.2
42.6
127
35.2
35.3
° Not detected; concentration represented by one-half the detection limit.
* Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Phthalate Esters
>
I
Lab #/Samp. //Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS8600289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
63
6.25"
6.5"
7.45"
6.65"
7.45"
8.35"
8.35"
7.1"
8.4"
7.4"
12.55"
7.55"
6.45"
7.55"
17.6"
7.4"
7.05"
12.3"
16.75"
14.4"
21.3"
6.9°
17.75"
12.55"
6.1"
8.45"
15.05°
77.5°
6.7"
19.15"
20.2"
64
58.9
6.4"
7.35"
6.55"
7.4"
8.25"
119
7"
27. 7l
7.35"
12.4"
7.45"
6.35"
27.8
17.35°
7.3"
6.95°
12.15"
16.55°
14.25°
21.05"
6.85"
17.55°
12.4°
6.05°
8.35°
14.85°
76.5°
6.6°
18.9°
19.95"
65
28.8
17'
31. 4<
25.4
20.1
17. 91
23
831
120
6.05°
41.7
41.1
5.25"
114
110
82.1
41.4
119
107
82.9
17.35"
18.5
14.45"
56.2
24.6
30.5
12.2"
132
21.7
15.6"
60.8
66
19. 11
25
77.9
53.5
13.7'
35.1
41.2
30.6
85.8
6.7"
93.9
42.4
5.8"
142
221
102
84.3
59.5
111
79.1
19.25"
12.9
16°
57.4
24.8
59.6
13.55"
157
24
17.3°
114
Compound # (see page A-l)
67
5.55"
85.8
284
164
118
185
122
26700
1500
1328
31.6
246
505
1180
5640
67.9
795
1980
467
178
91.2
25.7
49.7
32.6
102
208
117
7120
63.2
67.1
18.1"
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Phthalate Esters (cont.)
I
K-»
to
Compound # (see page A-l)
Lab #/Samp. #/Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
6.
13
20
16.
8
14
18.
19
19
6
18
13
12
20
12
19
14
12.
13
63
65°
.7"
.6"
85n
.2°
.4°
15"
.7"
.6"
.8"
.6°
.5°
.8"
.9"
.6°
.4°
.3°
75"
.5"
6
13
20.
16.
27
14.
17
19.
19.
6
18.
13.
12.
20.
12.
19.
14.
12
13.
64
.6n
.5n
35"
65"
.6
25°
.9°
45°
35"
.7"
35"
35n
65°
65"
45n
15n
15n
.6"
35°
67
49
88
65
.3
.8
65
.7
107
113
15
17
15
10
42
25
15.
26
71
75
47
16n
.9n
.5
.1"
11"
.4n
.6
.1
75"
.7
.3
.8
66
63.9
34.1
141
79
148
214
50.5
17.75n
17.65°
6.1n
16.75n
12. 2n
11.55°
18.85°
23.1
17.5°
60.1
65.1
55.9
67
5.95
49.2
0
146
15.1
18.2
31.5
38.5
17.6
17.5
61.5
16.65
12.1
259
262
30
17.35
D
0
n
n
0
n
12.8°
25.4
12.1
n
n Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Phosphate Triesters
>
u>
Compound t (see page A-l)
Lab #/Samp. #/Batch
17903
17905
17906
17908
17909
17910
17911
17912
17913
17914
17916
17919
17921
17922
17923
17924
17925
17926
17927
17928
17930
17931
17932
17934
17935
17937
17938
17939
17942
17944
17946
ACS8600387
ACS8600298
ACS8600467
ACS8600378
ACS8600092
ACS8600449
ACS8600412
ACS8600485
ACS8600136
ACS8600396
ACS8600154
ACS8600289
ACS8600430
ACS8600270
ACS8600494
ACS8600421
ACS8600458
ACS8600252
ACS8600029
ACS8600476
ACS8600074
ACS8600190
ACS8600038
ACS8600172
ACS8600519
ACS8600369
ACS8600323
ACS8600225
ACS8600065
ACS8600243
ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
68
26.5"
27.55"
31.65"
28.3°
31.75"
35.5"
35.55"
30.2"
35.65"
31.55"
53.5"
32.05"
27.4"
32.15"
74.5"
31.4"
29.95"
52.5"
71"
61.5"
90.5"
29.4"
75.5"
53.5°
25.95"
36"
64"
330°
28.45°
81.5"
86"
69
31.9"
33
.2°
38.1°
34.
38.
42
42.
05°
25°
.7°
75"
36.35"
42
38
38
37
36
85
.9"
38°
64°
.6°
33°
.7°
90°
.8°
.1°
63°
.5°
74°
109"
35
64
31.
43.
397
34.
103
.4°
91"
.5"
25"
35°
77°
.5°
25°
98°
.5"
31.
32
37.
33.
37
42
42
35.
42
37.
63
38.
32
38.
88
37.
35.
84
72
107
34
89
63
30.
42
70
45°
.7"
55"
55°
.7"
.1"
.1°
85"
.3"
45"
.5"
05"
.5"
15"
.5"
25"
55"
62"
.5"
.5"
.5"
.9"
.5"
.5"
85"
.7"
76°
392°
33.
96
75"
.5"
102°
11.
11
27
12.
13.
15.
15.
13.
71
45°
.9°
.4
25"
75°
35°
35"
05"
276
13.
23.
13.
11.
13
32
13.
12.
22
30
26.
39
12
32
23
11.
15.
27
142
12
35
37.
65"
05"
85"
85"
.9"
.3"
55°
95"
.6"
.8"
45"
.2"
.7"
.6°
.1"
25"
55"
.6"
.5"
.3"
.2"
15°
11.
11.
13
11
13.
14
14
12
14.
13.
22
13.
11
13
31
13
12
21.
29.
25
37.
12.
31
22.
10
26
137
11.
33
35
72
05°
45°
.2°
.8°
25°
.8"
.8°
.6°
85°
15"
.2"
35"
.4"
.4"
.1"
.1"
.5"
75°
65°
.5°
75°
25°
.4°
25°
.8°
15°
.6°
.5°
85°
.9°
.8°
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Phosphate Triesters (cont.)
I
H
^
Compound # (see page A-l)
Lab #/Samp. #/ Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
68
28.35"
58°
87. 5n
71.5°
34.85n
61.5°
77°
83.5°
83n
28.85n
79°
57.5"
54.5°
89°
53. 5n
82.5"
61"
54"
57.5"
69
34.15°
70°
105.5°
86.5°
42°
74°
93"
100.5"
100°
34.75°
95°
69°
65.5"
107"
64.5"
99.5°
73.5°
65°
69°
33.
70
65
69
104
41
72
91
99
34.
85
.4
.5
.5
.5
99
25
n
n
n
n
n
n
n
n
n
n
94"
68°
64
105
63
72
64
.5
.5
.5
98
.5
.5
68
n
n
n
n
n
n
n
12.
25.
37
30.
15.
26
33
36.
35.
12
34.
24
23
38
23
35.
26
23
24
71
25°
15°
.9"
95°
05°
.5°
.3"
15"
95°
.5"
15"
.8°
.5°
.4°
.2°
65"
.3°
.4°
.8°
27
24
36
29.
14
25
32
34.
34.
32
23
22.
22.
34.
25.
22.
23
72
.7l
.2°
.5°
85°
.5"
.5"
.1"
85"
65°
12°
.9°
.9°
65"
37"
35"
35°
35°
55°
.9°
n Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = PAHs
Compound # (see
Lab #/Samp. #/Batch
17903
17905
17906
17908
17909
17910
17911
17912
17913
17914
17916
17919
17921
17922
17923
17924
17925
17926
17927
17928
17930
17931
17932
17934
17935
17937
17938
17939
17942
17944
17946
ACS8600387
ACS8600298
ACS8600467
ACS8600378
ACS8600092
ACS8600449
ACS8600412
ACS8600485
ACS8600136
ACS8600396
ACS8600154
ACS8600289
ACS8600430
ACS8600270
ACS8600494
ACS8600421
ACS8600458
ACS8600252
ACS8600029
ACS8600476
ACS8600074
ACS8600190
ACS8600038
ACS8600172
ACS8600519
ACS8600369
ACS8600323
ACS8600225
ACS8600065
ACS8600243
ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
41
31.6
12. 6l
6.45"
41.8
25
7.25"
17.5'
6.15"
16. 11
24.3
15.8
6.55"
26.2
6.55"
15.25"
72.5
15.7
20.5
18.7
6.25"
22.2
12.9
15.4
40.2
11.4
25.6
14.9
102
2.9"
14.5
23.2
42
5.8"
6.05"
6.95"
6.2"
6.95"
7.75"
7.75"
6.6"
7.8"
6.9"
5.85"
7"
6"
7.05"
16.35"
6.85"
6.55"
5.7"
7.8"
6.7"
3.305"
3.215"
2.75"
5.85"
2.84"
3.94"
3.495"
36.1"
3.11"
2.97"
3.135"
43
5.65°
5.85"
6.75"
6"
6.75"
7.55"
7.55"
6.45"
7.6"
6.7"
5.65"
6.8"
5.85"
6.85"
15.9°
6.7"
6.4"
5.55"
7.6"
6.5"
3.215"
3.13"
2.675"
5.7"
2.765"
3.83"
3.4"
35.1"
3.025"
2.89"
3.045"
44
6.4"
6.65"
7.65"
6.85"
7.7°
8.6"
8.6"
7.3"
8.6"
7.65"
6.45"
7.75"
6.65"
7.8"
18.1"
7.6"
7.25"
6.3"
8.6"
7.4°
3.655"
3.56"
3.045"
6.45"
3.14"
4.355"
3.865"
39.95"
3.44"
3.285"
3.465"
45
5.85"
6.05"
6.95"
6.25"
7"
7.8"
7.8"
6.65"
7.85"
6.95"
5.85°
7.05"
6.05°
7.1"
16.45"
6.9"
6.6"
5.75"
7.85"
6.75"
3.33"
3.24"
6. 48'
12. 9l
6.751
3.965"
3.52"
36.35"
3.135"
2.99"
3.155"
46
5.65°
5.85°
6.75°
6"
6.75"
7.55°
7.55"
6.45°
7.6"
6.7"
5.65"
6.8°
5.85°
6.85°
15.9°
6.7°
6.4"
5.55"
7.6"
6.5"
3.215°
3.13°
2.675°
5.7°
2.765"
3.83"
3.4"
35.1"
3.025°
2.89"
3.045"
page A-l)
47
5.35"
5.6°
6.4"
5.75"
6.45"
7.2"
7.2"
6.15"
7.25"
6.4"
5.4"
6.5"
5.55°
6.5"
15.15"
6.35"
6.1"
5.3"
7.2"
6.2"
3.065"
2.98"
2.55"
5.4"
2.635"
3.65"
3.24"
33.5"
2.885"
2.755"
2.905"
48
5.55"
5.75°
6.6"
5.9"
6.65°
7.4°
7.4°
6.3°
7.45"
6.6"
5.55"
6.7"
5.7"
6.7"
15.6"
6.55"
6.25"
5.45"
7.45°
6.4°
3.155°
3.07°
2.625"
5.55"
2.71°
3.755"
11.7
34.45"
2.97°
2.835"
2.99"
49
5.15°
5.35°
6.15°
5.5"
6.2"
6.9°
6.9"
5.9"
6.95°
6.15°
5.2"
6.25"
5.35°
6.25°
14.55°
6.1"
5.85"
5.1°
6.95°
5.95°
2.945°
2.865°
2.45"
5.2°
2.53"
3.505"
3.115°
32.15"
2.77"
2.645"
2.79°
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = PAHs (cont.)
Compound # (see
Lab #/Samp. if/Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
41
12.8
9.99
16
18
16.3
17.2
13.8
12.8
15.4
26.1
13.1
68.7
13.1
33
13.7
8.72'
9.94
9.87
17.4
42
3.105"
3.18n
3.195"
3.92"
3.815"
3.35"
2.8105"
3.05"
3.035"
3.16"
2.88"
3.14"
2.975"
3.24"
2.935"
3.005"
3.33"
2.965"
3.14"
43
3.015"
3.095"
3.105"
3.81"
3.71"
3.26"
2.732"
2.965"
2.95"
3.07"
2.8"
3.055°
2.895"
3.15"
2.855"
2.925"
3.235"
2.88"
3.055"
44
3.43"
3.52"
3.535"
4.335"
4.22"
3.705"
3.1075"
3.375"
3.355°
3.495"
3.185"
3.475"
3.29"
3.58°
3.245°
3.325°
3.68"
3.275"
3.475"
45
3.125°
3.205"
3.22"
3.945°
3.84°
7.461
2.829°
3.07"
3.055°
3.18°
2.9°
3.165°
2.995°
3.26°
2.955°
3.03°
3.35°
2.985°
3.16°
46
3.015°
3.095"
3.105"
3.81"
3.71"
3.26"
2.732"
2.965°
2.95°
3.07°
2.8"
3.055"
2.895"
3.15"
2.855°
2.925°
7.211
2.88°
3.055°
page A-l)
47
2.875"
2.95"
2.96"
3.635"
3.535"
3.105"
2.605°
2.83°
2.815°
2.93°
2.67"
2.915"
2.76"
3.005"
2.72°
2.79°
3.085°
2.745°
2.91"
48
2.96°
3.035°
3.05°
3.74°
12.8
3.195°
2.6805°
2.91°
2.895°
3.015°
2.75°
2.995"
2.84"
3.09"
2.8"
2.87°
3.175°
2.825°
2.995°
49
2.765"
2.835"
2.845"
3.49"
3.4"
2.985"
2.5025°
2.715°
2.705°
2.815"
2.565"
2.8"
2.65"
2.885"
2.615"
2.68"
2.965"
2.64"
2.795"
" Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Other (quantitative)
>
I
Lab #/Samp. //Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS8600289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
28
5.1°
5.3°
6.1°
5.45°
6.1°
6.8"
6.8n
5.8°
6.85"
6.05°
5.1°
6.15"
5.25°
6.15"
14.35°
6.05°
5.75°
5°
6.85n
5.9°
2.9°
2.825°
2.415°
5.15°
2.495°
3.46°
3.07°
31.7°
2.73°
2.61°
2.75°
29
6.15°
6.4°
7.35°
6.55n
7.35°
8.2°
8.2°
7°
8.25°
7.3°
6.15°
7.4°
6.35°
7.45n
17.3°
7.25°
6.95"
6.05°
8.25°
7.1°
3.495°
3.405°
2.91°
6.2°
3.005°
4.165°
3.695°
38.2°
3.29n
3.14n
3.315°
30
6.3°
6.55°
7.5°
6.7°
7.55°
8.4°
8.4°
7.15°
8.45°
7.5°
6.35°
7.6n
6.5°
7.65°
17.75°
7.45°
7.1"
6.2°
8.45°
7.25°
3.585°
3.49°
2.985"
6.35°
3.08"
4.27"
3.79"
39.2°
3.375°
3.22"
3.4°
31
5.45"
5.65°
6.5°
5.8°
6.5"
7.25"
7.25"
6.2°
7.3°
6.45"
5.45"
6.55"
5.6"
6.6"
15.3"
6.45"
6.15"
5.35°
7.3°
6.3"
3.095"
3.015"
2.575°
5.45°
2.66°
3.69"
3.275"
33.85"
2.915"
2.78°
2.935"
Compound
32
6.55°
6.8°
7.8°
7°
7.85°
8.75°
8.75°
7.45°
8.8°
7.8°
6.6°
7.9°
6.75°
7.95°
18.45°
7.75°
7.4°
6.45°
8.8"
7.55°
3.73°
3.63°
3.105°
6.6°
3.21°
4.445°
3.945°
40.8"
3.515°
3.355°
3.54°
# (see page A-l)
33
25.3
5.9°
6.8°
12.9'
20
7.6°
7.6"
6.5"
7.65"
23.1
18.2
24.9
49.8
6.9"
93.2
33.8
13. 9l
23.2
23.2
6.55°
12.6
19.1
23.1
39.3
14.6
51.2
16.4
35.4°
3.05"
28.1
14.5
34
295
86.3
19. 8l
178
481
78.6
7.65"
94.2
110
299
163
230
548
86.9
785
660
345
284
192
192
428
391
303
323
212
732
298
365
3.06"
435
167
35
5.95°
6.2°
7.1°
6.35°
7.15°
7.95°
7.95°
6.8"
8"
7.1°
6°
7.2°
6.15°
7.2°
16.8"
7.05"
6.75°
5.85"
8"
6.9°
3.39°
3.3°
2.825°
6°
2.915°
4.04°
3.585°
37.05°
3.19°
3.05"
3.215°
36
5.9°
6.1"
7.05°
6.3"
7.05"
7.9°
7.9°
6.7°
7.9"
7°
5.9°
7.1"
6.1°
7.15°
16.6°
6.95°
6.65°
5.8°
7.9°
6.8°
3.355"
3.265°
2.79°
5.95°
2.885°
3.995°
3.545°
36.65°
3.155°
3.015"
3.18°
37
5.6°
5.85"
6.7"
6°
6.75"
7.55°
7.55°
6.4°
7.55"
6.7°
5.65"
6.8"
5.8°
6.8°
15.85°
6.65"
6.35°
5.55°
7.55"
6.5°
3.205°
3.12°
2.665°
5.65°
2.755°
3.82°
3.39°
35°
3.015°
2.88°
3 . 04° '
38
166
6.1"
7°
6.25"
7.05°
7.85°
7.85"
23.3
60.7
7"
5.9°
7.1°
6.05°
7.1°
16.55°
6.95°
6.65°
22.9
7.9°
6.75°
3.34°
3.25"
2.78°
5.9"
15.2
3.98"
27
36.5"
3.145°
3°
19.4
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Other (quantitative) (cont.)
I
H
00
Lab #/Samp. #/Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
28
2.725n
2.795°
2.805°
3.44°
3.35°
2.945°
2.467°
2.68°
2.665°
2.775°
2.53°
2.76°
2.615°
2.845°
2.575°
2.64°
2.925°
2.6°
2.755°
29
3.285°
3.365°
3.38°
4.145°
4.035°
3.545°
2.9725°
3.225°
3.21°
3.34°
3.05°
3.325°
3.15°
3.425°
3.105°
3.18°
3.52°
3.135°
3.32°
30
3.365°
3.45°
3.465°
4.25°
4.14°
3.635°
3 . 048°
3.31°
3.29°
3.425°
3.125°
3.41°
3.23°
3.515°
3.185°
3.26"
3.61"
3.215"
3.405"
31
2.905°
2.98°
2.995°
3.67°
3.575"
3.14"
2.632"
2.855"
2.845°
2.96°
2.7°
2.945°
2.785°
3.035°
2.75"
2.815°
3.12"
2.775"
2.94"
Compound
32
3.505°
3.595°
3.61°
4.425°
4.305°
3.835°
3.1725°
3.445°
3.425°
3.565°
3.255°
3.545°
3.36°
3.655°
3.315°
3.395"
3.76°
3.345°
3.545°
# (see page A-l)
33
20.6
23.1
16.1
9.09
13.6
17.8
20
16.8
20.6
33.4
22.9
13.2
12.7
25.9
33.6
18
12.1
18.6
29.8
34
262
52
163
69
149
146
305
195
287
277
345
198
208
313
344
175
122
492
299
35
3.185°
3.265°
3.28°
4.02°
3.915°
3.44"
2.8835"
3.13"
3.115°
3.24°
2.955°
3.225°
3.055°
3.325"
3.01°
3.085°
3.415°
3.04°
3.22°
36
3.15°
3.23°
3.245°
3.975°
3.87"
3.4°
2.851°
3.095°
3.08°
3.205°
2.925"
3.185°
3.02°
3.285°
2.98°
3.05°
3.38°
3.005°
3.185°
37
3.01°
3.085°
3.1°
3.8°
3.7°
3.25°
2.724°
2.955°
2.94°
3.06°
2.795°
3.045°
2.885°
3.14°
2.845°
2.915°
3.225°
2.87°
3.045°
38
3.135°
3.215°
3.23°
3.96"
3.855"
3.385°
2.84"
3.085"
3.065"
3.195°
2.915°
3.175°
3.005°
3.275°
2.965°
3.04°
9.631
9.241
3.175°
" Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
I
M
VO
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Other (quantitative) (cont.)
Compound # (see page A-l]
Lab #/Samp. //Batch
17903
17905
17906
17908
17909
17910
17911
17912
17913
17914
17916
17919
17921
17922
17923
17924
17925
17926
17927
17928
17930
17931
17932
17934
17935
17937
17938
17939
17942
17944
17946
ACS8600387
ACS8600298
ACS8600467
ACS8600378
ACS8600092
ACS8600449
ACS8600412
ACS8600485
ACS8600136
ACS8600396
ACS8600154
ACS8600289
ACS8600430
ACS8600270
ACS8600494
ACS8600421
ACS8600458
ACS8600252
ACS8600029
ACS8600476
ACS8600074
ACS8600190
ACS8600038
ACS8600172
ACS8600519
ACS8600369
ACS8600323
ACS8600225
ACS8600065
ACS8600243
ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
39
5.6"
5.85"
6.7"
6"
6.75"
7.55"
7.55"
6.4"
7.55"
6.7"
5.65"
6.8"
5.8"
6.8°
15.85°
6.65"
6.35"
5.55"
7.55"
6.5"
3.205"
3.12"
2.67"
5.65°
2.755"
3.82"
3.39°
35.05°
3.02"
2.88"
3.04"
40
6.3"
24.6
7.5"
6.7"
7.55"
8.4"
8.4"
85.1
8.45"
7.5"
6.35°
16.3'
15.5
23.2
44.6
39.7
7.1"
6.2"
8.45"
78.8
114
71.9
53.4
34
31.8
22
180
79. 7l
3.375"
63.9
39.7
73
13.15"
13.7°
15.7"
14.05"
15.75"
17.6°
17.6"
15°
17.7°
15.65°
26.45°
15.9°
13.6"
15.95"
37.1"
15.6"
14.9"
25.95"
35.35"
30.4"
45"
14.6"
37.45"
26.5"
12.9"
17.85"
31.7"
164"
14.1"
40.45"
42.65"
74
11.6"
12.1"
13.85"
12.4"
13.95"
15.55"
15.55"
13.25"
•15 . 6"
13.85"
23.35"
14.05"
12"
14.1"
32.75"
13.75"
13.15"
22.9"
31.2°
26.85"
39.75°
12.9°
33.05"
23.4"
11.4"
15.8"
28"
144.5"
12.45"
35.7"
37.65"
75
1.37°
1.425°
1.64"
1.465"
1.645°
1.835°
1.835°
1.565"
1.845°
1.635°
2.76"
1.66"
1.42"
1.665"
3.87"
1.625"
1.55"
2.705"
3.685"
3.17"
4.7"
1.52"
3.9"
2.75"
1.345"
1.865"
3.3"
17.1"
1.47"
4.215"
4.45"
76
9.35"
9.75"
11.2"
10"
11.25"
12.55°
12.55"
10.7"
12.6°
11.15°
18.85°
11.35°
9.7°
11.35°
26.4°
11.1°
10.6°
18.45°
25.2°
21.65°
32.05°
10.4°
26.65"
18.9"
9.2"
12.75°
22.6°
116.5°
10.05°
28.8°
30.4"
77
14.3"
14.9"
17.1"
15.25"
17.15"
19.15"
19.15"
16.3"
19.25"
17.05"
28.8"
17.3"
14.8"
17.35"
40.35"
16.95"
16.2"
28.2"
38.45"
33.05"
48.95"
15.85"
40.75"
28.85"
14.05"
19.45°
34.5°
178.5"
15.35"
44"
46.4"
78
5.5
15.1
6.55
5.9
202
7.35
7.35
6.25
7.4
6.55
11.05
127
5.7
n
t
n
n
n
n
n
n
n
n
n
6.7°
15.5
6.5
6.25
10.85
14.8
12.7
1820
6.1
15.65
11.1
5.4
7.5
194
68.5
43
16.9
n
n
n
n
n
n
n
n
n
n
n
n
n
17.85°
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Oroup = Other (quantitative) (cont.)
to
o
Compound # (see
Lab #/Samp. #/Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
39
3.01"
3.09n
3.1n
3.805"
3.7"
3.25"
2.7265"
2.96"
2.945"
3.065"
2.795"
3.05"
2.885"
3.145"
2.85"
2.92"
3.23"
2.875"
3.045"
40
11.1
18.1
83.3
312
153
14.6
32.8
138
36.8
31.3
17
98
99.5
67.4
39
22.9
3.61"
32.5
16.1
73
35. 2l
28.9"
43.5"
35.55"
17.3"
30.4"
38.25"
41.5"
41.3"
14.35"
39.25"
28.5"
27"
44.1"
26.65"
40.95"
30.2"
26.9"
28.5"
74
12.45"
25.5"
38.4"
31.4"
15.3"
26.85"
33.75"
36.65"
36.5"
12.65"
34.65"
25.15"
23.85"
38.95"
23.5"
36.15"
26.7"
23.75"
25.15"
1
3
4.
3
1.
3
3
4
4
1.
4
2.
2.
4.
2.
4
3
2.
2
75
.47"
.01"
535"
.71"
805"
.17"
.99"
.33"
.31"
495"
.09"
975"
815"
595"
775°
.27"
.15"
805"
.97"
76
10.05"
20.55"
31"
25.35"
12.35"
21.65"
27.25"
29.55"
29.4"
10.2"
27.95"
20.3"
19.25"
31.4"
18.95"
29.15"
21.5"
19.15"
20.3"
page A-l)
77
15.3"
31.4"
47.3"
38.7"
18.85"
33.1"
41.6"
45.15"
44.95"
15.6"
42.65"
31"
29.35"
47.95"
28.95"
44.5"
32.85"
29.25"
31"
78
5.9"
12.1"
18.2"
14.9"
7.25"
12.7"
16°
150
17.35"
6"
460
125
52.2
18.45"
1010
17.1"
12.65"
25.3
11.9"
" Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) fro» the FY86 MEATS (Unadjusted for Surrogate Recoveries)
Group = PCBs
to
H*
Compound # (see
Lab #/Samp. #/Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS8600289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
50
4.57°
4.755°
5.45"
4.88n
5.5n
6.1°
6.1°
5.2°
6.15"
5.45"
4.6°
5.55°
4.725n
5.55°
12.9"
5.4"
5.15°
4.51°
6.15°
5.3n
5.2°
5.05°
4.34n
9.2°
4.48°
6.2°
5.5°
57°
4.905n
4.685"
4.945n
51
4.625°
4.81°
5.55°
4.94°
5.55°
6.2°
6.2°
5.3°
6.2°
5.5°
4.655°
5.6°
4.785°
5.6°
13.05°
5.5°
5.25°
4.565°
6.2°
5.35°
5.3°
5.15°
4.39°
9.35°
4.535°
6.3°
5.6°
57.5°
4.965°
4.74°
5°
52
6.25°
6.5°
7.45°
6.65°
39.4
8.35°
8.35°
28.2
8.4°
7.45°
6.3°
25.5
8.75°
7.55°
17.6°
30
7.05°
28.1
8.4°
28.1
30.5
10°
5.95°
12.6°
6.1°
8.5°
14.9°
78°
6.7n
6.4°
6.75°
53
31.7
93.1
35.2
15.8
287
15.5
64.2
135
7.85°
45.9
83.9
149.5°
108
119
14.45°
191
66.6
92.5
6°
178
223
131
35.8°
9°
74.3
37
61°
55.5°
44.3
53.5
155
54
22.5
68.3
28.8
10.25°
465
12.85°
126
279
12.9°
27.3
252
612
285
68.2
27.05°
382
74
34.9
47.1
339
382
275
130
139
131
107
131
119.5°
63.9
102
152
55
334
394
145
65.1
1435
31.8
367
460
66.7
273
627
1006
785
474
28°
672
460
476
67.4
644
982
545
352
211
326
101
461
123.5°
139
199
985
page A-l)
56
131
183
36.5
10.9°
587
13.65°
164
135
13.7°
100
255
1149
358
215
28.75°
304
259
177
28.6
280
413
221
176
22.9°
146
35.8
266
127°
44
59.6
373
57
9.9°
52.5
11.85°
10.6°
188
13.3°
13.3°
12.95°
13.35°
11.8°
27.9
413
171
53.2
28°
131
123
52.1
13.35°
85.8
156
81.4
47.5
20°
83.4
13.5°
177
123.5°
10.65°
10.15°
149
58
10°
22.1
11.9°
10.65°
82.9
13.35°
13.35°
23.4
13.4°
11.9°
20.6
119
93.9
12.1°
28.15°
95.4
28.3
21.8
13.4°
11.55°
83.5
24.5
9.45°
20.1°
21.4
13.55°
52.3
124.5°
10.7°
10.25°
10.8°
59
12 . 65°
37
15.1°
13.5°
65.1
16.95°
16.95°
43.2
17°
15.05°
12.75°
86.7
107
15.35°
35.7°
95
14.3°
34.1
17°
45.6
72.9
31.8
12°
25.5°
59.3
17.2°
64
157.5°
13.6°
12.95°
49.5° '
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 MEATS (Unadjusted for Surrogate Recoveries)
Group = PCBs (cont.)
I
CO
to
Compound # (see
Lab #/Samp. #/Batch
17947 ACS8600500
17948 ACS8600350
17949 ACS8600216
17951 ACS8600261
17953 ACS8600305
17955 ACS8600145
17956 ACS8600118
17958 ACS8600341
17959 ACS8600127
17960 ACS8600181
17962 ACS8600083
17965 ACS8600332
17967 ACS8600109
17968 ACS8600207
17969 ACS8600047
17970 ACS8600234
17986 ACS8600314
17987 ACS8600056
17988 ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
50
4.895°
5"
5.05°
6.2°
6°
5.3°
4.43°
4.81°
4.785°
4.98"
4.545"
4.955"
4.695°
5.1"
4.63"
4.74"
5.25"
4.67°
4.95°
51
4.955"
5.1"
5.1n
6.25°
6.1"
5.35"
4.485°
4.87°
4.845"
5.05"
4.6"
5°
4.75°
5.15"
4.685"
4.8"
5.3"
4.73"
5°
52
6.7°
23
35.8
8.45°
8.2"
7.2"
38.9
42.6
48.1
15.3'
9.85"
9.65"
25.4
28.9
7.55"
7.4"
7.2"
6.4"
6.75"
53
37
101
203
6.05"
5.85"
5.15°
200
125
330
90.4
142
64°
141
164
46.5"
45.1"
33.55"
41.4°
4.83"
54
76
212
436
175
12.6°
78.6
407
115
503
267
414
271
360
350
177
184
123
217
134
55
206
274
611
243
13.05"
385
553
484
659
528
580
578
419
935
304
366
239
259
236
page A-l)
56
85.6
67
214
28
13.45°
158
201
106
247
117
174
259
130
382
68.8
84
43.2
42.8
47.1
57
10.65"
23.9
16.45°
13.4"
13.05°
13.15°
99.1
20.9
150
11.6°
16.8°
39.6
10.2°
234
10.05°
10.3°
11.4°
10.15°
10.75°
58
10.7°
10.95°
11°
13.5°
13.15°
11.55"
15.35"
10.5°
27.25°
10.9°
9.9°
19.9"
10.25"
19.95"
10.1°
10.35°
11.45°
10.2°
10.8°
59
13.55°
13.9"
14.3"
17.1°
16.65°
14.65°
15.3"
68.2
60.5°
13.8°
12.6°
24°
13°
33
12.8°
13.15°
14.55°
12.95°
13.7°
Not detected; concentration represented by one-half the detection limit.
reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Pesticides (qualitative)
N)
U)
Compound
Lab #/Samp. I/Batch
17903
17905
17906
17908
17909
17910
17911
17912
17913
17914
17916
17919
17921
17922
17923
17924
17925
17926
17927
17928
17930
17931
17932
17934
17935
17937
17938
17939
17942
17944
17946
ACS8600387
ACS8600298
ACS8600467
ACS8600378
ACS8600092
ACS8600449
ACS8600412
ACS8600485
ACS8600136
ACS8600396
ACS8600154
ACS8600289
ACS8600430
ACS8600270
ACS8600494
ACS8600421
ACS8600458
ACS8600252
ACS8600029
ACS8600476
ACS8600074
ACS8600190
ACS8600038
ACS8600172
ACS8600519
ACS8600369
ACS8600323
ACS8600225
ACS8600065
ACS8600243
ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
85
10
2.5"
10
100
2.5"
2.5"
10
10
2.5"
10
2.5"
2.5"
10
2.5"
10
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
86
2.5"
2.5"
2.5"
2.5"
2.5n
2.5"
2.5"
2.5"
60
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
98
30
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
10
2.5"
10
30
2.5"
2.5"
2.5"
10
2.5"
2.5"
30
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
40
2.5"
10
99
10
5"
10
5"
10
5"
10
5"
10
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
100
10
200
10
2.5"
2.5"
2.5"
2.5°
2.5"
10
100
2.5"
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5°
2.5°
2.5"
40
2.5"
2.5"
2.5"
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
f (see page A-l)
101
2.5"
50
2.5"
2.5°
2.5°
2.5°
2.5"
300
2.5°
40
2.5"
2.5"
2.5"
2.5"
2.5°
2.5°
2.5°
2.5"
2.5"
2.5°
2.5°
2.5°
2.5°
2.5°
2.5°
2.5"
300
2.5"
2.5°
2.5"
2.5°
102
5°
5°
5°
5"
5"
5°
5°
5°
5"
5°
5"
5"
5"
5"
5"
5"
5"
5°
5°
5°
5°
5°
5°
5°
5"
5°
5"
5"
5"
5"
5"
106
2.5°
2.5°
2.5°
2.5"
2.5"
2.5°
2.5°
100
2.5"
2.5"
2.5°
2.5°
40
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5°
2.5°
2.5°
2.5°
300
2.5°
2.5°
2.5°
2.5°
107
5°
5"
5"
5"
5°
5°
5°
5°
5"
5°
5"
5°
5°
5°
5°
5°
5°
5°
5°
5°
5°
5°
5n
5°
5°
5"
5°
5"
5"
5"
5°
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Pesticides (qualitative) (cont.)
>
to
Compound
Lab #/Samp. //Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
85
2.5n
2.5n
2.5"
2.5"
2.5"
2.5n
2.5n
2.5"
2.5°
2.5°
2.5°
2.5°
2.5n
2.5"
2.5n
2.5n
2.5n
2.5n
2.5°
86
2.5"
2.5"
2.5"
2.5"
2.5°
2.5n
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5"
2.5n
2.5n
2.5°
2.5"
2.5"
2.5"
98
2.5"
20
2.5"
2.5"
2.5"
2.5"
2.5"
2.5n
2.5"
2.5"
10
2.5"
10
20
2.5"
10
2.5"
20
2.5"
99
5"
5n
5"
5"
5n
5°
5n
5"
5"
5"
5"
5"
5"
5"
5"
5"
5°
5"
5°
100
2.5"
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
# (see page A-l)
101
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5°
2.5°
2.5°
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
102
5"
5"
5"
5°
5"
5°
5°
5°
5°
5°
5°
5°
5°
5°
5°
5"
5"
5"
5"
106
2.5°
2.5°
2.5°
2.5"
2.5"
2.5"
2.5°
2.5°
2.5°
2.5°
2.5°
2.5°
2.5°
2.5°
2.5°
2.5"
2.5"
2.5"
2.5"
107
5°
5"
5"
5"
5"
5"
5"
5n
5°
5°
5°
5°
5°
5"
5"
5°
5°
5°
5°
" Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Chlorinated aromatics (qualitative)
to
01
Compound # (see page A-l)
Lab #/Samp. //Batch
17903
17905
17906
17908
17909
17910
17911
17912
17913
17914
17916
17919
17921
17922
17923
17924
17925
17926
17927
17928
17930
17931
17932
17934
17935
17937
17938
17939
17942
17944
17946
ACS8600387
ACS8600298
ACS8600467
ACS8600378
ACS8600092
ACS8600449
ACS8600412
ACS8600485
ACS8600136
ACS8600396
ACS8600154
ACS8600289
ACS8600430
ACS8600270
ACS8600494
ACS8600421
ACS8600458
ACS8600252
ACS8600029
ACS8600476
ACS8600074
ACS8600190
ACS8600038
ACS8600172
ACS8600519
ACS8600369
ACS8600323
ACS8600225
ACS8600065
ACS8600243
ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
88
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
5°
5n
5n
5°
5n
5n
5°
5n
5"
5n
5°
5n
5n
5n
89
5n
5n
5°
5°
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5°
5n
5n
5n
5"
5°
5n
5n
5n
5°
5"
5n
5n
5n
5"
90
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5»
5n
5n
5n
5"
5n
5"
91
5n
5n
5n
5"
5n
5°
5n
5°
5n
5n
5n
5n
5°
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
5n
5"
5n
5n
5n
5n
5n
5n
92
5n
5°
5n
5n
5"
5n
5"
5°
5n
5n
5n
5"
5n
5n
5n
5n
5°
5n
5°
5n
5n
5n
5n
5n
5n
5n
5n
5n
5°
5"
5n
95
5n
5n
5n
5°
5n
5°
5n
10
5n
5n
5°
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
5n
5"
96
2.5°
2.5n
2.5n
2.5°
2.5°
2.5n
2.5°
2.5"
2.5°
2.5"
2.5"
2.5"
2.5n
2.5n
2.5"
2.5"
2.5"
2.5°
2.5n
2.5°
2.5n
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5n
2.5"
2.5"
97
5°
5°
5n
5°
5n
5n
5n
60
5°
5n
5°
5n
5°
5°
5"
5°
5°
5n
5°
5n
5D
200
5"
5n
5n
5"
5n
5n
5n
5°
5n
110
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5"
5n
5°
5°
5n
5n
5n
5n
5n
5°
20
5n
5n
5n
5°
5°
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Chlorinated aromatics (qualitative) (cont.)
I
to
ON
Compound # (see page A-l)
Lab #/Samp. #/Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
88
5n
5n
5n
5n
5°
5°
5n
5n
5"
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
89
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5"
5n
5n
5n
5°
5n
5n
5n
5n
90
5n
5n
5n
5n
5"
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5°
5°
91
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
92
5n
5"
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
95
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
5n
5°
5n
5n
5"
96
2.5n
2.5n
2.5n
2.5°
2.5°
2.5n
2.5°
2.5n
2.5°
2.5°
2.5n
2.5°
2.5°
2.5°
2.5°
2.5n
2.5°
2.5n
2.5n
97
5n
5n
5n
5n
5n
5n
5n
5"
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
5n
110
5n
5n
5"
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5n
n Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = PAHs (qualitative)
Lab #/Samp. #/Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS8600289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
105
2.5°
2.5°
2.5°
2.5n
2.5n
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5n
2.5n
2.5n
2.5"
2.5"
2.5n
2.5°
2.5"
2.5"
2.5n
2.5n
2.5°
2.5°
2.5"
2.5"
2.5°
2.5"
2.5°
2.5"
108
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
30
2.5"
2.5"
2.5"
2.5"
20
2.5"
2.5"
10
2.5"
2.5"
2.5"
2.5"
7
10
2.5"
' 2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
109
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.S°
300
2.5"
2.5"
2.5"
10
2.5"
2.5"
2.5°
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
Compound # (see page A-l)
111
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 KEATS (Unadjusted for Surrogate Recoveries)
Group = PARs (qualitative) (cont.)
to
00
Lab #/Samp. #/Batch
17947 ACS8600500
17948 ACS8600350
17949 ACS8600216
17951 ACS8600261
17953 ACS8600305
17955 ACS8600145
17956 ACS8600118
17958 ACS8600341
17959 ACS8600127
17960 ACS8600181
17962 ACS8600083
17965 ACS8600332
17967 ACS8600109
17968 ACS8600207
17969 ACS8600047
17970 ACS8600234
17986 ACS8600314
17987 ACS8600056
17988 ACS8600403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
105
2.5"
2.5°
2.5"
10
2.5"
2.5"
10
10
10
10
10
10
10
10
10
10
10
10
2.5"
108
2.5"
2.5n
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
109
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5"
2.5"
2.5°
2.5"
Compound # (see page A-l)
111
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
° Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Other (qualitative)
to
vo
Compound # (see page A-l)
Lab f/Samp. //Batch
17903 ACS8600387
17905 ACS8600298
17906 ACS8600467
17908 ACS8600378
17909 ACS8600092
17910 ACS8600449
17911 ACS8600412
17912 ACS8600485
17913 ACS8600136
17914 ACS8600396
17916 ACS8600154
17919 ACS8600289
17921 ACS8600430
17922 ACS8600270
17923 ACS8600494
17924 ACS8600421
17925 ACS8600458
17926 ACS8600252
17927 ACS8600029
17928 ACS8600476
17930 ACS8600074
17931 ACS8600190
17932 ACS8600038
17934 ACS8600172
17935 ACS8600519
17937 ACS8600369
17938 ACS8600323
17939 ACS8600225
17942 ACS8600065
17944 ACS8600243
17946 ACS8600163
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
4
4
79
400
300
300
500
300
400
10°
20
70
400
100
500
10"
200
10"
10°
10"
100
70
10"
70
80
10°
10n
10"
10°
10°
10°
10°
100
10"
80
20
10
2.5"
20
30
10
2.5"
2.5n
10
30
2.5"
10
2.5n
2.5"
2.5n
2.5°
2.5"
2.5"
2.5n
2.5°
20
20
40
30
2.5"
20
20
200
2.5"
10
2.5n
81
30
20
70
60
100
100
100
2.5n
40
30
20
100
100
20
40
40
100
60
100
60
20
30
70
100
30
200
40
30
10
2.5"
2.5n
82
60
20
90
100
100
2.5°
2.5"
40
2.5n
50
10
40
800
90
200
300
500
400
2.5°
2.5"
20
20
2.5n
60
10
200
2.5n
100
2.5°
70
100
83
5n
5n
5n
5°
5°
5n
5n
5n
5°
5°
5°
5n
5n
5n
20
5°
5n
20
20
5n
5n
5°
5°
5n
5n
5°
5°
20
5°
5n
5n
84
5n
5n
5"
5n
5»
5°
5n
5n
5°
5°
5n
5n
5°
5n
5n
5n
5°
5n
5n
5°
5°
5°
5°
5n
5n
5n
5°
5n
5n
5°
5n
87
5°
5n
5n
5n
5n
5°
5"
100
5°
5"
5°
5n
5n
400
5n
5°
5n
5n
5°
5°
5n
5n
5n
20
5n
5°
5n
5°
5"
5n
5n
93
10°
10°
10°
10°
10°
10°
10°
10°
10°
10°
10°
10°
10"
10n
10"
10°
10"
10°
10°
10°
10°
10°
10°
10°
10°
10°
10°
10°
10°
10°
10n
94
5n
5n
5n
5n
5°
5n
5n
100
5n
5°
5"
5°
5"
5n
5°
5°
5°
5n
5°
5n
5n
5°
5n
5n
5n
5n
5n
5n
5n
5n
5n
103
5°
5"
5n
5D
5°
5°
5°
5n
5n
5n
5n
5n
5n
5n
5n
5n
5°
5n
5n
5n
5°
5°
5n
5°
5n
5n
5n
5n
5n
5n
5n
104
5n
5n
5"
5n
5n
5n
5n
5n
5n
5n
40
90
5°
100
5n
60
5n
5n
80
5n
5n
5n
2.5"
5°
5n
5n
5n
5°
5n
5n
5n
-------
Listing of Lipid-Adjusted Concentrations (ng/g) from the FY86 NHATS (Unadjusted for Surrogate Recoveries)
Group = Other (qualitative) (cont.)
I
U)
o
Compound # (see page A-l)
Lab #/Samp. #/Batch
17947
17948
17949
17951
17953
17955
17956
17958
17959
17960
17962
17965
17967
17968
17969
17970
17986
17987
17988
ACS8600500
ACS8600350
ACS8600216
ACS8600261
ACS8600305
ACS8600145
ACS8600118
ACS8600341
ACS8600127
ACS8600181
ACS8600083
ACS8600332
ACS8600109
ACS8600207
ACS8600047
ACS8600234
ACS8600314
ACS8600056
ACS86Q0403
4
4
4
4
4
4
4
5
5
5
5
5
5
5
5
5
3
5
4
79
50
10"
10"
70
60
300
10"
10n
100
800
10n
10"
10"
30
10"
10"
10"
10"
50
80
2.5"
2.5"
2.5°
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5°
2.5"
2.5"
10
2.5"
2.5"
2.5"
2.5"
81
2.5"
90
100
2.5"
2.5"
2.5"
20
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
2.5"
82
30
200
400
300
40
300
100
80
90
90
200
2.5"
90
400
60
100
30
200
500
83
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
84
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
87
5"
5"
5"
5"
5"
5"
5"
5"
5"
30
5"
5"
5"
5"
5"
5"
5n
5"
5"
93
10"
10"
10"
10"
10"
10"
10"
10"
10"
10"
10"
10"
10°
10"
10"
10"
10°
10"
10"
94
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5°
5"
5"
5"
5"
5"
5"
5"
5"
103
5"
5"
5"
5"
5"
5"
5"
5"
5"
5n
5"
5"
5"
5"
5"
5n
5"
5"
5"
104
5"
5n
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5"
5°
5"
" Not detected; concentration represented by one-half the detection limit.
1 Trace reading.
-------
APPENDIX B
Listing of NHATS FY86 QC Data for Compounds Detected in
At Least 50% of Composites (plus Octachlorobiphenyl)
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = p,p-DDT (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
'S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 9.770
ND 9.770
ND 4.890
ND 4.010
ND 4.890
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
4.885
4.885
2.445
2.005
2.445
210.000
240.000
232.000
259.000
263.000
508.000
456.000
468.000
644.000
623.000
254.000
271.000
284.000
353.000
333.000
Adj .
Cone.
(ng/g)
4.885
4.885
2.445
2.005
2.445
185.942
210.435
203.904
225.948
229.214
444.422
402.054
411.417
555.027
538.255
225.644
239.411
250.200
306.497
290.153
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-l
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = p,p-DDE (m/z=288) (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
- S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 10.200
ND 10.200
ND 5.090
ND 5.090
ND 5.090
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
5.100
5.100
2.545
2.545
2.545
3000.00
2170.00
1980.00
5100.00
4750.00
2750.00
1580.00
1230.00
5390.00
5300.00
1370.00
2390.00
1900.00
5120.00
4610.00
Adj .
Cone.
(ng/g)
5.100
5.100
2.545
2.545
2.545
2652.68
1975.03
1819.90
4367.22
4081.47
2469.79
1514.67
1228.30
4624.61
4551.65
1327.15
2159.77
1759.96
4388.87
3972.46
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-2
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = p,p-DDE (m/z=316) (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
. MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual. (ng/g)
ND 10.200
ND 10.200
ND 5.090
ND 5.090
ND 5.090
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
5.100
5.100
2.545
2.545
2.545
2860.00
2070.00
1100.00
5150.00
4410.00
2760.00
1530.00
623.000
5420.00
4840.00
1340.00
2250.00
1750.00
5130.00
4330.00
Adj .
Cone.
(ng/g)
.
.
.
•
2525.03
1880.04
1088.08
4394.70
3790.53
2443.39
1439.16
698.637
4615.14
4141.60
1284.03
2027.00
1618.77
4378.37
3725.21
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-3
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = HEPTACHLOR EPOXIDE (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual. (ng/g)
ND 9.780
ND 9.780
ND 4.890
ND 4.890
ND 4.890
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
.PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
4.890
4.890
2.445
2.445
2.445
66.700
117.000
129.000
131.000
144.000
241.000
255.000
209.000
344.000
353.000
125.000
146.000
204.000
199.000
192.000
Adj .
Cone.
(ng/g)
4.890
4.890
2.445
2.445
2.445
56.412
92.211
100.751
102.174
111.427
193.800
203.840
170.720
266.725
273.458
101.226
116.073
157.505
153.914
148.918
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-4
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = TRANS-NONACHLOR (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 10.000
ND 10.000
ND 5.000
ND 5.000
ND 5.000
PQ
PQ
PQ
PQ-
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
5.000
5.000
2.500
2.500
2.500
174.000
168.000
541.000
251.000
227.000
434.000
85.000
309.000
562.000
566.000
137.000
235.000
362.000
316.000
276.000
Adj .
Cone.
(ng/g)
5.000
5.000
2.500
2.500
2.500
157.942
153.043
457.579
220.809
201.214
385.973
101.123
283.557
490.030
493.683
131.655
211.550
315.421
277.825
245.151
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
1Concentration is above the upper calibration limit
3=Compound not analyzed
B-5
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = BETA-BHC (unspiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data
Qual.
ND
ND
ND
ND
ND
ND
PQ
PQ
PQ
ND
PQ
PQ
ND
ND
PQ
PQ
PQ
PQ
PQ
PQ
LOD
(ng/g)
11.300
11.300
5.630
5.630
5.630
11.600
.
.
•
11.500
•
.
5.590
5.780
.
.
.
.
.
•
Unadj .
Cone.
(ng/g)
5.650
5.650
2.815
2.815
2.815
5.800
202.000
277.000
476.000
5.750
425.000
403.000
2.795
2.890
342.000
374.000
369.000
329.000
393.000
35.200
Adj .
Cone.
(ng/g)
5.650
5.650
2.815
2.815
2.815
19.842
180.029
241.262
403.736
19.801
362.097
344.135
17.388
17.466
294.332
320.458
316.376
283.718
335.970
43.845
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-6
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = OXYCHLORDANE
Fraction
(unspiked compound)
= 6%
Batch
1
2
3
4
5
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data
Qual.
ND
ND
ND
ND
ND
ND
ND
ND
PQ
ND
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
LOD
(ng/g)
11.900
11.900
5.950
5.950
5.850
• 12.200
12.100
12.000
,
12.200
.
.
.
.
•
.
.
.
•
•
Unadj .
Cone.
(ng/g)
5.950
5.950
2.975
2.975
2.925
6.100
6.050
6.000
150.000
6.100
162.000
175.000
149.000
135.000
143.000
180.000
188.000
151.000
184.000
166.000
Adj .
Cone.
(ng/g)
5.950
5.950
2.975
2.975
2.925
12.475
12.435
12.394
129.962
12.475
139.760
150.374
129.146
117.716
124.247
154.456
160.987
130.779
157.722
143.026
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-7
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound « DIELDRIN (CORRECTED) (spiked compound)
Fraction - 50%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Numbe r
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual. (ng/g)
ND
ND
ND
,
ND
ND
TR
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
ND
PQ
PQ
TR
PQ
Unadj .
Cone.
(ng/g)
24
24
24
24
24
60
32
32
165
41
183
229
142
383
24
136
145
25
274
.200
.200
.200
.200
.850
.500
.500
.900
.000
.000
.000
.000
.000
.000
.450
.000
.000
.500
.000
Adj.
Cone .
(ng/g)
•
,
•
24
54
31
31
139
38
154
191
120
317
24
115
123
25
228
.919
.026
.165
.492
.344
.105
.040
.597
.566
.330
.593
.667
.015
.450
.337
LOD/ 2
LOD/ 2
LOD/ 2
3
LOD/ 2
LOD/ 2
LOD/ 2
MB=Method Blank, C=Control, Si-High spike, S2-Low spike
PQ-Positive quantifiable, TR=Trace, ND-Not detected
LOD=Detection Limit
Unadj. Cone.:
Adj. Cone.:
Concentrations are unadjusted for surrogate
recoveries.
Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2-Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
<-Compound not analyzed
B-8
-------
Listing of FY86 NHATS QC Data for Compound* Detected in
At Least 44% of Composites
Compound - 1,4-DICHLOROBENZENE (spiked compound)
Fraction • 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data
Qual .
ND
ND
ND
ND
ND
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
TR
PQ
PQ
LOD
(ng/g)
8.590
8.590
4.300
4.300
4.300
.
.
.
,
•
•
.
•
•
.
.
4.410
.
•
Unadj .
Cone.
(ng/g)
4.295
4.295
2.150
2.150
2.150
99.000
87.500
166.000
118.000
212.000
353.000
652.000
522.000
760.000
892.000
207.000
227.000
6.500
251.000
269.000
Adj .
Cone.
(ng/g)
4.295
4.295
2.150
2.150
2.150
131.002
116 .881
213.273
154.333
269.757
529.199
896.843
734 .744
1026.50
1190.71
285.079
309.002
39.237
339.250
361.264
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
MB=Method Blank, C»Control, Si-High spike, S2-Low spike
PQ=Positive quantifiable, TR-Trace, ND»Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2-Concentration replaced by one-half the detection limit
1-Concentration is above the upper calibration limit
3"Compound not analyzed
B-9
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = HEXACHLOROBENZENE (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual. (ng/g)
ND 9.810
ND 9.810
ND 4.910
ND 4.910
ND 4.910
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
4.905
4.905
2.455
2.455
2.455
75.200
66.600
76.300
68.400
69.800
264.000
292.000
253.000
310.000
300.000
82.500
112.000
125.000
145.000
126.000
Adj .
Cone.
(ng/g)
4.905
4.905
2.455
2.455
2.455
75.242
67.098
76.284
68.803
70.128
265.663
292.245
254.980
308.893
299.709
85.050
112.900
125.345
144.256
126.251
LOD/ 2
LOD/ 2
LOD/ 2
LOD/2
LOD/ 2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.:
Adj. Cone.:
Concentrations are unadjusted for surrogate
recoveries.
Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
^Concentration is above the upper calibration limit
3=Compound not analyzed
B-10
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = NAPHTHALENE (unspiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data
Qual.
ND
ND
ND
ND
ND
TR
ND
TR
ND
PQ
PQ
PQ
ND
ND
PQ
PQ
PQ
PQ
PQ
PQ
LOD
(ng/g)
9.690
9.690
4.850
4.850
4.850
10.100
9.850
10.300
9.650
»
*
•
4.810
4.980
.
.
.
.
.
.
Unadj .
Cone.
(ng/g)
4.845
4.845
2.425
2.425
2.425
15.500
4.925
14.200
4.825
11.500
9.720
13.700
2.405
2.490
10.600
12.500
12.500
10.900
11.800
9.690
Adj .
Cone.
(ng/g)
4.845
4.845
2.425
2.425
2.425
15.220
5.007
13.964
4.910
11.357
9.638
13.482
2.573
2.655
10.488
12.323
12.323
10.777
11.647
9.609
LOD/ 2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-ll
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = DI-N-BUTYL PHTHALATE (unspiked compound)
Fraction = 50%
Batch
1
2
3
4
5
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data
Qual .
PQ
ND
ND
PQ
ND
ND
PQ
PQ
ND
PQ
ND
ND
ND
PQ
PQ
PQ
PQ
PQ
PQ
LOD
(ng/g)
9.090
9.090
9.090
•
24.100
24.300
.
.
18.600
•
27.500
18.100
18.700
.
.
•
.
.
•
Unadj .
Cone.
(ng/g)
44.900
4.545
4.545
.
13.700
12.050
12.150
46.000
58.000
9.300
71.700
13.750
9.050
9.350
57.700
62.500
78.600
20.200
54.600
104.000
Adj .
Cone.
(ng/g)
44.900
4.545
4.545
.
13.700
13.481
13.571
44.062
54.871
11.004
67.211
15.012
10.778
11.049
54.600
58.924
73.426
20.822
51.808
96.306
LOD/ 2
LOD/2
3
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-12
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = BUTYL BENZYL PHTHALATE (spiked compound)
Fraction = 50%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
PQ
ND 10.100
ND 10.100
10.100
PQ
ND 21.100
PQ
ND 30.500
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
ND 20.700
PQ
PQ
Unadj .
Cone.
(ng/g)
29.100
5.050
5.050
,
14.000
10.550
75.000
15.250
70.100
13.700
52.300
215.000
57.400
333.000
244.000
97.100
153.000
10.350
156.000
123.000
Adj .
Cone.
(ng/g)
29.100
5.050
5.050
a
14.000
12.881
70.935
17.115
66.521
15.718
65.644
212.285
69.891
318.056
238.261
94.611
144.852
16.532
147.691
117.950
LOD/ 2
LOD/ 2
3
LOD/ 2
LOD/2
LOD/ 2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-13
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = BIS (2-ETHYLHEXYL) PHTHALATE
Fraction = 50%
(unspiked compound)
Batch
1
2
3
4
5
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data LOD
Qual . (ng/g)
PQ
PQ
PQ
10.000
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
ND 19.700
PQ
PQ
ND 20.200
PQ
Unadj .
Cone.
(ng/g)
205.000
581.000
288.000
.
15.400
57.800
83.100
1170.00
560.000
45.600
97.000
222.000
55.400
293.000
34.200
9.850
151.000
348.000
10.100
1670.00
Adj .
Cone .
(ng/g)
205.000
581.000
288.000
.
15.400
72.462
95.252
1074.29
524.825
61.473
107.772
220.367
70.301
284.322
51.204
29.271
156.413
333.863
29.496
1524.67
3
LOD/2
LOD/2
1
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-14
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = TETRACHLOROBIPHENYLS
Fraction = 6%
(spiked compound)
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 8.000
ND 8.000
ND 8.000
ND 8.000
ND 8.000
ND 80.700
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
4.000
4.000
4.000
4.000
4.000
40.350
124.000
123.000
117.000
134.000
551.000
620.000
613.000
895.000
938.000
205.000
249.000
175.000
324.000
348.000
Adj .
Cone.
(ng/g)
4.000
4.000
4.000
4.000
4.000
35.748
97.682
96.942
92.500
105.086
453.460
504.775
498.458
707.026
739.838
167.544
199.828
145.496
255.716
273.445
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-15
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = PENTACHLOROBIPHENYLS (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 17.200
ND 17.200
ND 17.200
ND 17.200
ND 17.200
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
8.600
8.600
8.600
8.600
8.600
67.100
303.000
329.000
325.000
142.000
466.000
531.000
795.000
1120.00
1232.00
270.000
281.000
187.000
438.000
736.000
Adj .
Cone.
(ng/g)
8.600
8.600
8.600
8.600
8.600
67.483
247.165
266.969
263.923
124.533
427.195
477.026
676.513
923.749
1010.43
235.967
243.932
172.977
364.023
590.950
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-16
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = HEXACHLOROBIPHENYLS (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 17.800
ND 17.800
ND 17.800
ND 17.800
ND 17.800
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
8.900
8.900
8.900
8.900
8.900
1100.00
1361.00
1224.00
1261.00
1331.00
1460.00
1606.00
1572.00
1379.00
1545.00
1208.00
1237.00
1130.00
1315.00
1328.00
Adj .
Cone.
(ng/g)
8.900
8.900
8.900
8.900
8.900
923.747
1122.55
1018.20
1046.38
1099.70
1243.17
1354.64
1327.45
1180.19
1307.74
1017.30
1039.05
958.072
1098.87
1108.73
LOD/ 2
LOD/ 2
LOD/ 2
LOD/2
LOD/ 2
1
1
1
1
1
1
1
1
1
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR-Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-17
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = HEPTACHLOROBIPHENYLS (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 18.300
ND 18.300
ND 18.300
ND 18.300
ND 18.300
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
9.150
9.150
9.150
9.150
9.150
566.000
948.000
1029.00
665.000
866.000
1577.00
1766.00
1848.00
2465.00
2676.00
1021.00
1249.00
1373.00
1055.00
1146.00
Adj .
Cone.
(ng/g)
9.150
9.150
9.150
9.150
9.150
489.736
780.702
842.399
565.144
718.243
1371.55
1516.15
1575.42
2044.75
2208.22
864.094
1036.94
1132.67
890.176
959.375
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
1
1
1
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-18
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = OCTACHLOROBIPHENYLS (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 17.800
ND 17.800
ND 17.800
ND 17.800
ND 17.800
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
Unadj .
Cone.
(ng/g)
8.900
8.900
8.900
8.900
8.900
97.100
280.000
146.000
219.000
80.600
931.000
1773.00
1533.00
2324.00
2429.00
365.000
549.000
775.000
690.000
747.000
Adj .
Cone.
(ng/g)
8.900
8.900
8.900
8.900
8.900
90.918
231.291
128.448
184.475
78.254
873.608
1520.65
1332.37
1938.65
2022.75
332.060
472.226
647.320
581.730
625.330
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
1
1
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.:
Adj. Cone.:
Concentrations are unadjusted for surrogate
recoveries.
Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
1Concentration is above the upper calibration limit
3=Compound not analyzed
B-19
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = O-CYMENE (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data
Qual.
ND
ND
ND
ND
ND
ND
ND
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
ND
TR
ND
PQ
PQ
LOD
(ng/g)
10.200
10.200
5.100
5.100
5.100
10.500
10.100
.
,
•
.
.
.
•
10.300
9.990
5.230
.
•
Unadj .
Cone.
(ng/g)
5.100
5.100
2.550
2.550
2.550
5.250
5.050
19.000
11.400
18.300
77.000
15.300
105.000
13.500
14.500
5.150
10.800
2.615
11.300
13.100
Adj .
Cone.
(ng/g)
5.100
5.100
2.550
2.550
2.550
5.140
4.960
17.525
10.679
16.895
88.547
33.077
113.338
30.813
32.176
9.719
14.670
7.513
15.290
16.892
LOD/ 2
LOD/2
LOD/ 2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.-. Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-20
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = D-LIMONENE (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data LOD
Qual . (ng/g)
ND 10.200
PQ
ND 5.120
ND 5.120
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
PQ
TR 5.260
PQ
PQ
Unadj .
Cone.
(ng/g)
5.100
27.900
2.560
2.560
19.500
92.900
85.400
186.000
112.000
164.000
134.000
239.000
193.000
285.000
261.000
120.000
117.000
7.530
150.000
148.000
Adj .
Cone.
(ng/g)
5.100
27.900
2.560
2.560
19.500
90.572
83.817
174.433
107.777
154.616
143.621
238.293
196.400
279.180
257.955
118.972
116.151
17.729
146.021
144.203
LOD/ 2
LOD/ 2
LOD/ 2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-21
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = OCTAMETHYL-CYCLOTETRASILOXANE (spiked compound)
Fraction = 6%
Batch
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
1
2
3
4
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17974
17977
17980
17983
17972
17975
17978
17981
17984
17973
17976
17979
17982
17985
Sample
Type
MB
MB
MB
MB
MB
C
C
C
C
C
SI
SI
SI
SI
SI
S2
S2
S2
S2
S2
Data
Qual.
ND
ND
PQ
ND
ND
ND
ND
PQ
ND
PQ
ND
PQ
PQ
PQ
PQ
ND
ND
ND
PQ
PQ
LOD
(ng/g)
11.300
11.300
f
5.640
5.640
11.600
11.200
•
5.780
•
11.500
•
•
•
•
11.400
11.100
5.790
.
•
Unadj .
Cone.
(ng/g)
5.650
5.650
156.000
2.820
2.820
5.800
5.600
20.300
2.890
9.140
5.750
88.200
112.000
31.800
54.700
5.700
5.550
2.895
7.440
15.100
Adj .
Cone .
(ng/g)
5.650
5.650
156.000
2.820
2.820
5.374
5.194
18.435
2.753
8.382
19.479
93.828
114.861
42.540
63.516
8.806
8.566
6.337
10.396
17.282
LOD/ 2
LOD/ 2
LOD/ 2
LOD/ 2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.:
Adj. Cone.:
Concentrations are unadjusted for surrogate
recoveries.
Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-22
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = 1-NONENE (unspiked compound)
Fraction = 50%
Batch
1
2
3
4
5
1
.1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data LOD
Qual . (ng/g)
D
D
ND 20.000
ND 20.000
ND 20.000
D
D
D
D
ND 20.000
D
ND 20.000
D
D
D
D
D
D
D
D
Unadj .
Cone.
(ng/g)
600.000
1000.00
10.000
10.000
10.000
200.000
400.000
500.000
600.000
10.000
20.000
10.000
800.000
800.000
1000.00
600.000
700.000
90.000
300.000
1000.00
Adj .
Cone.
(ng/g)
600.000
1000.00
10.000
10.000
10.000
209.984
390.136
480.212
570.288
38.839
47.846
38.839
750.441
750.441
930.593
570.288
660.365
110.900
300.060
930.593
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-23
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = 1,2,4-TRIMETHYLBENZENE (unspiked compound)
Batch
1
2
3
4
5
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data
Qual.
ND
ND
D
ND
ND
ND
D
D
D
D
D
D
D
ND
ND
D
D
D
D
ND
Unadj .
LOD Cone .
(ng/g) (ng/g)
5.000 2
5.000 2
40
5.000 2
5.000 2
5.000 2
40
10
20
100
80
30
30
5.000 2
5.000 2
100
100
30
10
5.000 2
.500
.500
.000
.500
.500
.500
.000
.000
.000
.000
.000
.000
.000
.500
.500
.000
.000
.000
.000
.500
Adj .
Cone.
(ng/g)
2
2
40
2
2
4
38
11
20
92
74
29
29
4
4
92
92
29
11
4
.500
.500
.000
.500
.500
.628
.407
.384
.392
.453
.437
.399
.399
.628
.628
.453
.453
.399
.384
.628
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-24
-------
Listing of FY86 NHATS QC Data for Compounds Detected in
At Least 44% of Composites
Compound = HEXYL ACETATE
Fraction
(unspiked compound)
50%
Batch
1
2
3
4
5
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
Lab.
Number
17901
17915
17929
17943
17957
17971
17972
17973
17974
17975
17976
17977
17978
17979
17980
17981
17982
17983
17984
17985
Sample
Type
MB
MB
MB
MB
MB
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
C
SI
S2
Data LOD
Qual . (ng/g)
D
ND 5.000
D
ND 5.000
ND 5.000
D
D
D
ND 5.000
D
D
ND 5.000
D
D
D
D
D
D
D
D
Unadj .
Cone.
(ng/g)
20.000
2.500
400.000
2.500
2.500
50.000
50.000
100.000
2.500
400.000
100.000
2.500
400.000
30.000
100.000
70.000
400.000
60.000
60.000
50.000
Adj .
Cone.
(ng/g)
20.000
2.500
400.000
2.500
2.500
52.995
52.995
98.033
10.208
368.261
98.033
10.208
368.261
34.979
98.033
71.010
368.261
62.002
62.002
52.995
LOD/2
LOD/2
LOD/2
LOD/2
LOD/2
MB=Method Blank, C=Control, Sl=High spike, S2=Low spike
PQ=Positive quantifiable, TR=Trace, ND=Not detected
LOD=Detection Limit
Unadj. Cone.: Concentrations are unadjusted for surrogate
recoveries.
Adj. Cone.: Concentrations are adjusted for surrogate
recoveries.
Codes for final column
LOD/2=Concentration replaced by one-half the detection limit
l=Concentration is above the upper calibration limit
3=Compound not analyzed
B-25
-------
APPENDIX C
Plots of Observed vs. Spiked Concentrations
for Spiked Semivolatile Compounds Detected in
At Least 50% of Composites (plus Octachlorobiphenyl)
Plots of Observed Concentration vs. Batch ID
for Unspiked Semivolatile Compounds Detected in
At Least 50% of Composites
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=P.P-DDT
600
500 «•
0
b
s
e
r
v
e
d
A
d
J
C
o
n
c
e
n
t
r
a
t
i
o
n
400
300 «•
200
100
0 «•
I
-20 0 20 40 60 80 100 120 KO 160 180
Spiked Concentration
NOTE: 5 obs had missing values. 1 obs hidden.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
200
220
-------
o
to
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=P.P-DDE (UNAOJ.)
5000
0
b
s
e 4000 +
r
v
e
d
A
d 3000
j
A 5
2000
1000
0
30
60 90 120 150 180
210 240
270
300
Spiked Concentration
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
o
w
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUND=P,P-DDE (M/Z=316)
5000
0 4500
b
s
e
r
v
e
d
4000
3500
A
d
j
3000
2500
2000
1500
1000
500 +
-30
0
30
60
90
120
150
180
210
240
270
300
Spiked Concentration
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=HEPTACHLOR EPOXIDE
300
o
I
250 *
0
b
s
e
r
v
e
d
A
d
j
200
150 «•
34
5
100 *
50
34
2
-20 0 20 40 60 SO 100 120 140 160
Spiked Concentration
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch 10. Observed cones, are adjusted for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUND=TRANS-NONACHLOR
o
Ol
500
0
b
s
e 400
r
v
e
d
A
d 300
j
200
12
100 «•
0 «•
...4.....
-20
20 40 60 80 100 120 140
Spiked Concentration
*•--
160
180
200
220
2AO
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch ID. -Observed cones, are adjusted for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44X of NHATS FY86 Composites
COMPOUNDEDIELDRIN (CORRECTED)
350
300 «•
o
o\
0
b
s
e
r
V
e
d
A
d
j
C
o
n
c
e
n
t
r
a
t
i
0
n
250
200
150
100
50
2
34
14
.4. +
0 20
40 60 80
100 120 140 160 180 200 220 240
Spiked Concentration
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted-for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44X of NHATS FY86 Composites
COMPOUND*1,4-DICHLOROBENZENE
1200 *
1000
?
0
b
s
e
r
v
e
d
A
d
j
C
o
n
c
e
n
t
r
a
t
i
o
n
800
600
400
200
-100 0 100 200 300 400 500 600 700 800 900 1000
Spiked Concentration
NOTE: 5 obs had missing values. 1 obs hidden.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
1100
1200
1300
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=HEXACHLOROBENZENE
350
o
00
300
250
A
d 200
j
150
C
o
n
c
e
n
t
r
a 100
t
i
o
50
4
35
13
24
0 +
J
-20 0 20 40 60 80 100 120 140 160 180
Spiked Concentration
NOTE: 5 obs had missing values. 1 obs hidden.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
200
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUNDS- CYMENE
120
100
o
1
to
0
b
s
e
r
V
e 80 +
d
A
d
j
60 •<
C
o
n
c
e
n
t 40 <
r
a
t
i
o
n
2
4 5
20
>
-30
35
4
12
0 30
5
24
13
60 90
120 150 180 210 240 270 300
Spiked Concentration
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
h»
o
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUND=D-LIMONENE
300
250
200
150
100
50
-20
20
40
60
80
160
180
200
100 120 140
Spiked Concentration
NOTE: 5 obs had missing values. 1 obs hidden.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
220
240 260
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semi volatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUND=OCTAMETHYL-CYCLOTETRASILOXANE
160
140
120
A 100
d
j
80
60 +
20
5
124
4
213
0 +
-20
0
20
40
60 80
100
120
140
160
180 200
220
Spiked Concentration
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUND=TETRACHLOROBIPHENYLS
800
700
0
M
10
0
b
s
e
r 600
V
e
d
A 500
d
j
C 400
0
n
c
e
n 300
t
r
a
t
i 200
0
n
100
3 2
50
100
150
200 250 300
Spiked Concentration
350
400
450
500
..«. 4...
550 600
NOTE: 5 obs had missing values. 3 obs hidden.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUND=PENTACHLOROBIPHENYLS
1000
o
I
H
W
0
b
s
e
r
v
e
d
A
d
j
c
o
n
c
e
n
t
r
a
t
i
o
n
800
600
400 +
200
-35
0 35 70 105 140 175
210 245 280 315 350 385 420 455 490 525
560 595 630 665
Spiked Concentration
NOTE: 5 obs had missing values. 2 obs hidden.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
UOO
1200
o
H
*
0
b
s
e
2
5
3
r 1000 +
V
e
d
A
1
d 800
j
C
0
n 600 +
c
e
n
t
r
a 400 +
t
i
o
n
200 *
• -*-
-2
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44X of NHATS FY86 Composites
COHPOUND=HEXACHLOROBIPHENYLS
38
78
118
158
198
358
398
438
238 278 318
Spiked Concentration
NOTE: 5 obs had missing values. 3 obs hidden.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
478
S18
• •*-
558
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Conposites
COMPOUND=HEPTACHLOROBIPHENYLS
2500
2000
1500
o
1
Ul
c
o
n
c
e
n
t
r
a
t
i
0
n
1000
500
-70 0 70 140 210 280 350 420
NOTE: 5 obs had missing values. 1 obs hidden.
A90 560 630 700 770
Spiked Concentration
+ + * + ••• + + +.
SAO 910 980 1050 1120 1190 1260 1330
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semfvolatile Compounds
Detected in At Least AAX of NHATS FY86 Composites
COMPOUND=OCTACHLOROBIPHENYLS
2000
1750
o
1
H
0\
c
0
n
c
e
n
t
r
a
t
i
o
n
1500
A 1250 +
d
j
1000
750
500
250
0 «•
-2 98 198 298 398 498 598 698 798
Spiked Concentration
NOTE: 5 obs had missing values. 2 obs hidden.
898
998
1098
1198
1298
1398
Note:
Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
-------
Plots of Observed vs. Spiked Concentrations (ng/g) for Spiked Semivolatile Compounds
Detected in At Least 44% of NHATS FY86 Composites
COMPOUND=BUTYL BENZYL PHTHALATE
350
o
300
250
A
d 200
j
C
o
n 150
c
e
n
t
r
100
50
3 1
135
-20 0 20 40 60 80 100 120 140 160 180 ' 200
Spiked Concentration
NOTE: 5 obs had missing values.
Note: Plotting symbol is the Batch ID. Observed cones, are adjusted for surrogate recoveries.
220 240
-------
400
350
o
H
00
0
b
s
e
r 300
V
e
d
A 250
d
j
C 200
0
n
c
e
n 150
t
r
a
t
i 100
0
n
50
0 *
Plots of Observed Concentrations (ng/g, Adjusted for Surrogate Recoveries)
versus Batch ID for Unspiked Compounds Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=BETA-BHC
L H
I H
0.5
1.0
1.5
2.0
2.5
3.0
Batch ID
3.5
4.0
4.5
5.0
5.5
Plotting symbols: C=Control sample, L=Lou-spiked sample, H=High-spiked sample
-------
Plots of Observed Concentrations (ng/g. Adjusted for Surrogate Recoveries)
versus Batch 10 for Unspiked Compounds Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=OXYCHLORDANE
160
140
o
H
to
0
b
s
e
r
V
e
d
A
d
j
C
0
n
c
e
n
t
r
a
t
i
0
n
120
100
80
60
40
20
C L H
-.4...
2.5
4
3.0
Batch ID
..4...
5.0
0.5
1.0
1.5
2.0
3.5
4.0
4.5
5.5
Plotting symbols: C=Control sample, L=Lowspiked sample, H=High-spiked sample
-------
Plots of Observed Concentrations (ng/g, Adjusted for Surrogate Recoveries)
versus Batch ID for Unspiked Compounds Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=NAPHTHALENE
16
O
14
0
b
s
e
r 12
v
e
d
A
d 10 +
j
C
o
n 8 +
c
e
n
t
r
a 6 +
t
i
o
n
I H
L H
-.4...
4.0
0.5
1.0
1.5
2.0
2.5
3.0
Batch ID
3.5
4.5
5.0
5.5
Plotting symbols: C=Control sample, L=Low-spiked sample, H=Hfgh-spiked sample
-------
Plots of Observed Concentrations (ng/g. Adjusted for Surrogate Recoveries)
versus Batch ID for Unspiked Compounds Detected in At Least 44% of NHATS FY86 Composites
COMPOUNDED I-N-BUTYL PHTHALATE
100
0
b
s
e
r
v
e
d
80
A
d
j
60
O
C
o
n
c
e
n
t
r
a
t
i
o
n
20
C H
I H
..4.--
1.0
..4...
4.5
..4...
5.5
0.5
1.5
2.0
2.5
3.0
Batch ID
3.5
4.0
5.0
Plotting symbols: C=Control sample, L=Low-spiked sample, H=High-spiked sample
-------
o
I
10
to
1600 *
1400 +
0
b
s
e
r 1200 »
v
e
d
A 1000 *
d
j
C 800 *
o
n
c
e
n 600
t
r
a
t
i 400
o
n
200
Plots of Observed Concentrations (ng/g, Adjusted for Surrogate Recoveries)
versus Batch ID for Unspiked Compounds Detected in At Least 44X of NNATS FY86 Conposites
CONPOUNO=BIS (2-ETHYLHEXYL) PHTHALATE
C H
C H
0.5
1.0
1.5
2.0
2.5 3.0
Batch ID
3.5
4.0
4.5
5.0
5.5
Plotting synbols: C*Control sample, L=Low-spiked sample, H^High-spiked sample
-------
Plots of Observed Concentrations (ng/g. Adjusted for Surrogate Recoveries)
versus Batch 10 for Unspiked Compounds Detected in At Least 44X of HHATS FY86 Coaposites
COMPOUND*)-NONENE
1000 *
o
w
0
b
s
e 800 *
r
V
e
d
A
d 600 +
j
C
o
n
c 400 *
e
n
t
r
a
t
i 200 *
0
n
L H
0.5
1.0
1.5
2.0
2.5
3.0
Batch 10
3.5
4.0
4.5
5.0
5.5
Plotting symbols: C=Control sample, L*low-spiked sample, H=High-spiked sample
-------
Plots of Observed Concentrations (ng/g, Adjusted for Surrogate Recoveries)
versus Batch ID for Unspiked Compounds Detected in At Least 44X of NHATS FY86 Composites
COMPOUNDS, 2,4 - TRIHETHYLBEMZENE
100
L H
0
b
s
e
r
v
e
d
A
d
j
80
60
O
to
c
o
n
c
e
n
t
r
a
t
i
o
n
C H
20
0 +
0.5
1.0
1.5
2.0
2.5
3.0
Batch ID
3.5
4.0
4.5
5.0
5.5
Plotting symbols: C=Control sample, L=Low-spiked sample, H=High-spiked sample
-------
Plots of Observed Concentrations (ng/g. Adjusted for Surrogate Recoveries)
versus Batch 10 for Unspiked Compounds Detected in At Least 44X of NHATS FY86 Composites
COMPOUND=HEXYL ACETATE
400
350
0
1
10
U1
0
b
s
e
r 300
V
e
d
A 250
d
j
'
C 200
o
n
c
e
n 150
t
r
a
t
i 100
o
n
50
C H
C H
L
0.5
1.0
1.5
2.0
2.5
3.0
Batch ID
3.5
4.0
4.5
5.0
*•--
5.5
Plotting symbols: C=Control sample, L=Low-spiked sample, H=High-spiked sample
-------
APPENDIX D
Summary of QC Data for FY86 NHATS Spiked Semivolatile Compounds
Not on the Target List for Statistical Analysis
-------
Summary of QC Data for the FY86 NHATS spiked Compounds not on the Target List
D
Compound
O,P-DDT
GAMMA-CHLORDANE
MIREX
DIELDRIN (UN ADJ.)
1,2,4-
TRICHLOROBENZENE
Avg.
Spike
Spike # # Level
Level Samples Detected (ng/g)
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
5
5
5
5
5
5
5
5
5
5
5
5
4
5
5
5
5
5
5
5
0
0
0
0
0
0
5
5
0
2
5
5
0
2
3
4
0
0
4
5
^ ,
0.
69.
276.
—
0.
56.
224.
_
0.
54.
218.
—
0.
55.
220.
-
0.
52.
208.
00
48
65
00
35
34
00
84
30
00
34
32
00
31
24
Avg.
Observed
Cone.
(ng/g)
3
3
8
22
3
3
62
230
3
6
68
230
24
66
107
177
3
5
42
199
.60
.21
.10
.79
.57
.26
.20
.09
.50
.88
.96
.86
.20
.10
.68
.74
.35
.00
.81
.80
Background
Adjusted Std. Dev
Recovery of Cone.
(%) (ng/g)
^
-
7.04
7.07
—
-
104.51
101.11
_
—
113.10
102.69
—
-
75.39
50.72
—
-
72.41
93.60
1.
1.
1.
1.
1.
1.
11.
35.
1.
5.
18.
33.
0.
43.
84.
106.
1.
1.
20.
39.
41
15
06
45
40
15
93
31
37
16
64
88
00
72
47
80
31
93
56
93
•
c.v.
(%)
39.12
35.78
13.10
6.34
39.12
35.18
19.18
15.35
39.01
74.98
27.03
14.68
0.00
66.15
78.44
60.09
39.12
38.49
48.03
19.98
-------
Summary of QC Data for the FY86 NHAT8 Spiked Compounds not on the Target List (cont.)
Avg.
Spike
Spike t t Level
Compound Level Samples Detected (ng/g)
1,2,4,5-
TETRACHLOROBENZENE
DIETHYL PHTHALATE
TRIS (2-CHLOROETHYL)
PHOSPHATE
TRIPHENYL PHOSPHATE
PHENANTHRENE
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB .
Control
Low
High
5
5
5
5
4
5
5
5
4
5
5
5
4
5
5
5
5
5
5
5
0
0
5
5
0
3
4
4
0
0
0
0
0
0
2
3
0
2
5
5
.
0.
72.
289.
_
0.
58.
231.
—
0.
939.
3742
—
0.
48.
193.
.
0.
59.
237.
00
71
73
00
07
38
00
19
.4
00
47
15
00
58
42
Avg.
Observed
Cone.
(ng/g)
3.
4.
61.
255.
6.
19.
49.
115.
28.
50.
101.
296.
10.
18.
48.
100.
3.
5.
68.
245.
56
51
92
32
89
88
78
04
60
27
37
66
24
48
19
02
67
50
23
98
Background
Adjusted Std. Dev
Recovery of Cone.
(%) (ng/g)
.
-
78.88
86.62
_
-
51.36
41.28
—
—
5.47
6.58
—
-
61.23
42.38
_
-
105.35
101.30
1
1
9
29
2
10
43
88
0
21
13
10
0
7
39
82
1
1
8
24
.40
.68
.62
.42
.77
.72
.53
.62
.00
.84
.88
.91
.03
.85
.71
.09
.44
.78
.51
.20
c.v.
(*)
39.34
37.18
15.53
11.52
40.29
53.93
87.45
77.03
0.00
43.44
13.69
3.68
0.24
42.48
82.39
82.08
39.23
32.33
12.48
9.84
-------
summary of QC Data for the FY86 NHATS Spiked Compounds not on the Target List (cont.)
w
Avg.
Spike
Spike # # Level
Compound Level Samples Detected (ng/g)
CHRYSENE
BENZO (A) PYRENE
HEXACHLORO BUTADIENE
2-PHENYL PHENOL
MONOCHLOROBIPHENYLS
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
5
5
5
5
5
5
5
5
5
5
5
5
4
5
5
5
5
5
5
5
0
2
4
5
0
0
1
4
0
0
5
5
0
0
2
4
0
0
5
5
0
12
51
0
60
242
0
49
197
0
52
208
0
63
254
^m
.00
.83
.00
—
.00
.90
.45
_
.00
.48
.18
—
.00
.29
.24
—
.00
.93
.52
Avg.
Observed
Cone.
(ng/g)
3
7
14
57
3
3
9
46
3
3
31
150
4
8
23
91
4
3
56
233
.47
.06
.28
.16
.24
.21
.54
.48
.95
.61
.44
.11
.93
.54
.50
.70
.10
.95
.84
.10
Background
Adjusted Std. Dev.
Recovery of Cone. C.V.
(%) (ng/g) (%)
^^
-
56.45
98.12
—
-
10.38
17.74
_
—
56.27
74.39
_
-
28.65
39.75
_
-
82.68
90.01
1.36
4.24
6.84
12.66
1.27
1.23
11.52
48.39
1.55
1.39
4.54
28.00
0.00
3.78
16.85
61.94
0.00
0.06
6.00
18.24
39.
59.
47.
22.
39.
38.
120.
104.
39.
38.
14.
18.
0.
44.
71.
67.
0.
1.
10.
7.
12
97
92
15
12
16
80
11
22
52
44
65
00
26
69
54
00
51
55
82
-------
Summary of QC Data for the FY86 NHATS Spiked Compounds not on the Target List (cont.)
Avg.
Spike
Spike # # Level
Compound Level Samples Detected (ng/g)
DICHLOROBIPHENYLS
TRI CHLOROB I PHEN YLS
0
^ NONACHLOROBIPHENYLS
DECACHLOROBIPHENYL
D,L-ISOBORNEOL
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
MB
Control
Low
High
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
5
0
0
5
5
0
2
4
5
0
2
5
5
0
2
4
5
0
0
4
4
0.
70.
280.
_
0.
62.
247.
M
0.
388.
1549
_
0.
242.
966.
-
0.
67.
268.
00
49
68
00
11
48
00
81
.3
00
37
78
00
46
61
Avg.
Observed
Cone.
(ng/g)
4.
3.
65.
253.
5.
10.
61.
245.
8.
28.
502.
1730.
11.
19.
331.
1231.
3.
3.
24.
96.
15
77
88
88
60
60
85
86
95
81
79
29
35
78
82
57
74
57
01
15
Background
Adjusted Std. Dev
Recovery of Cone.
(%) (ng/g)
.
-
88.04
89.14
—
-
82.48
95.17
_
-
121.88
109.96
—
-
128.74
125.50
-
-
30.36
34.43
0.
0.
11.
24.
0.
4.
19.
37.
0.
23.
117.
487.
0.
9.
149.
372.
1.
1.
12.
45.
00
05
02
81
00
80
90
78
00
26
83
76
00
76
70
88
47
32
35
22
C.V.
0.00
1.45
16.73
9.77
0.00
45.27
32.18
15.37
0.00
80.73
23.43
28.19
0.00
49.31
45.12
30.28
39.23
36.94
51.41
47.03
-------
Summary of QC Data for tbe FY86 NHATS Spiked Compounds not on the Target List (cont.)
Avg.
Spike
Spike # # Level
Compound Level Samples Detected (ng/g)
D
1
01
2-INDANONE MB
Control
Low
High
COUMARIN MB
Control
Low
High
ETHYL HYDROCINNAMATE MB
Control
Low
High
5
5
5
5
5
5
5
5
4
5
5
5
0
0
0
0
0
0
0
0
0
0
3
4
0
43
174
0
63
253
0
82
328
—
.00
.73
.04
_
.00
.62
.52
-
.00
.59
.97
Avg.
Observed
Cone.
(ng/g)
3
3
6
14
3
3
7
20
11
21
66
167
.53
.51
.31
.92
.54
.46
.63
.18
.77
.13
.20
.64
Background
Adjusted Std. Dev
Recovery of Cone.
(%) (ng/g)
^ >
—
6.42
6.56
_
-
6.55
6.59
—
-
54.53
44.62
1.
1.
1.
1.
1.
1.
1.
1.
0.
9.
36.
81.
39
21
18
43
38
24
16
51
05
02
51
88
•
c.v.
(*)
39.23
34.48
18.62
9.59
39.12
35.96
15.23
7.47
0.42
42.67
55.15
48.84
-------
APPENDIX E
Characterizing the Distribution of NHATS FY86
Semivolatile Compound Concentrations (in ng/g,
Unadjusted for Surrogate Recoveries)
Based on All 50 Composite Samples
-------
Characterizing the Distribution of NHATS FY86 Semivolatile Compound
Concentrations (in ng/g, Unadjusted for Surrogate Recoveries) Based on All 50 Composite Samples(1)
Compound Number
and Name
Percent Avg .
Detected LOD
Avg.
Cone.
Minimum
Cone.®
Median
Cone.
Maximum
Cone.
PESTICIDES
1
2
3
3
4
5
6
7
8
9
10
11
12
13
14
15
16
60
60
61
62
P,P-DDT
O,P-DDT
P,P-DDE (M/Z=288)
P,P-DDE (M/Z=316)
O,P-DDE
O,P-DDD
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE )
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
OXYCHLORDANE
TRANS-NONACHLOR
GAMMA-CHLORDANE
MIREX
DIELDRIN
DIELDRIN (CORRECTED)
ENDRIN
ENDRIN KETONE
96
0
100
100
0
0
0
92
0
4
0
0
94
78
92
0
32
12
62
0
2
9.14
10.9
—
—
13.7
13.5
11.0
30.8
12.3
11.7
11.6
35.2
31.9
20.0
26.9
10.8
10.9
123.
146.
85.3
227.
5.46
3010.
2950.
6.87
6.75
5.50
209.
6.15
8.74
5.79
17.6
81.3
123.
161.
5.41
12.1
70.0
54.3
72.8
43.4
<5.88
<5.45
291.
273.
<6.86
<6.74
<5.49
<8.26
<6.14
<5.89
<5.71
<5.48
<13.2
<8.97
<11.2
<5.40
<5.41
<52.9
7.41
<65.6
<38.4
133
3.62
2290.
2020.
4.55
4.47
3.65
199.
4.08
3.91
3.79
3.64
80.2
140.
145.
3.59
6.15
59.0
36.2
67.5
39.8
1470.
35.7
11400.
14300.
45.0
44.2
36.0
581.
40.3
118.
37.5
600.
218.
366.
612.
35.4
51.6
337.
337.
417.
244.
CHLOROBENZENES
17
18
19
20
21
22
23
24
25
1 , 3-DICHLOROBENZENE
1 , 4-DICHLOROBENZENE
1 , 2-DICHLOROBENZENE
1,2, 3-TRICHLOROBENZENE
1,2, 4-TRICHLOROBENZENE
1,3, 5-TRICHLOROBENZENE
1 ,2,3, 4-TETRACHLOROBENZENE
1,2,3, 5-TETRACHLOROBENZENE
1,2,4, 5-TETRACHLOROBENZENE
0
86
0
0
0
0
0
0
0
10.1
16.7
10.3
11.8
10.2
11.1
11.7
11.6
10.8
5.04
78.4
5.14
5.88
5.08
5.53
5.84
5.79
5.38
<5.03
<4.97
<5.04
<5.87
<5.07
<5.52
<5.84
<5.78
<5.38
3.34
50.1
3.35
3.90
3.37
3.67
3.88
3.84
3.57
33.0
279.
33.0
38.5
33.3
36.2
38.3
37.9
35.3
-------
Characterizing the Distribution of NHATS FY86 Semivolatile Compound
Concentrations (in ng/g, Unadjusted for Surrogate Recoveries) Based on All 50 Composite Samples (cont.)
M
I
to
Compound Number
and Name
Percent Avg .
Detected LOD
Avg.
Cone.
Minimum
Cone . ®
Median
Cone.
Maximum
Cone.
CHLOROBENZENES ( cont . )
26
27
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
PENTACHLOROBENZENE
HEXACHLOROBENZENE
NAPHTHALENE
ACENAPHTHALENE
ACENAPHTHENE
FLUORENE
PHENANTHRENE
FLUORANTHRENE
PYRENE
CHRYSENE
BENZO (A) PYRENE
MONOCHLOROBIPHENYLS
D I CHLOROB I PHENYLS
TRICHLOROB I PHENYLS
TETRACHLOROB I PHENYLS
PENTACHLOROBIPHENYLS
HEXACHLOROBIPHENYLS
HEPTACHLOROB I PHENYLS
OCTACHLOROB I PHENYLS
NONACHLOROB I PHENYLS
DECACHLOROB I PHENYL
0
98
84
0
0
0
8
2
0
4
0
0
0
30
66
88
94
86
44
26
28
10.1
33.0
PAHs
13.6
11.0
10.7
12.2
11.1
10.7
10.2
10.7
9.81
PCBs
12.8
13.0
20.2
69.6
65.0
110.
65.8
33.9
32.3
43.7
5.04
54.7
.
20.5
5.51
5.36
6.09
5.92
5.44
5.11
5.61
4.91
6.41
6.49
16.5
88.1
188.
422.
176.
60.7
25.7
32.6
<5.03
15.0
<5.80
<5.50
<5.35
<6.09
<5.66
<5.35
<5.10
<5.25
<4.90
<8.68
<8.78
<11.9
<9.66
<20.5
<26.1
<21.8
<19.8
<18.9
<24.0
3.34
44.3
15.5
3.65
3.55
4.04
4.86
3.76
3.39
3.75
3.26
5.05
5.12
8.42
64.1
133.
376.
133.
18.4
13.4
17.0
33.0
199.
102.
36.1
35.1
39.9
36.3
35.1
33.5
34.4
32.1
57.0
57.5
78.0
330.
612.
1440.
1150.
413.
125.
158.
PHTHALATE ESTERS
63
64
65
DIMETHYL PHTHALATE
DIETHYL PHTHALATE
DI-N-BUTYL PHTHALATE
0
10
76
27.1
27.9
23.6
13.6
17.9
63.0
<12.2
<12. 1
<10.5
12.6
13.4
31.0
77.5
119.
831.
-------
Characterizing the Distribution of NHATS FY86 Semivolatile Compound
Concentrations (in ng/g, Unadjusted for Surrogate Recoveries) Based on All 50 Composite Samples
(cont.)
M
Compound Number
and Name
Percent Avg.
Detected LOD
Avg.
Cone.
Minimum
Cone.®
Median
Cone.
Maximum
Cone.
PHTHALATE ESTERS (cont.)
66
67
BUTYL BENZYL PHTHALATE
BIS (2-ETHYLHEXYL) PHTHALATE
72
78
26.6
27.4
58.0
1010.
<11.6
<11.1
41.8
76.8
221.
26700.
PHOSPHATE TRIESTERS
68
69
70
71
72
28
29
30
31
32
33
34
35
36
37
38
39
40
73
74
75
76
77
78
TRIBUTYL PHOSPHATE
TRIS (2-CHLOROETHYL) PHOSPHATE
TRIS ( 2 , 3-DIBROMOPROPYL )
PHOSPHATE
TRIPHENYL PHOSPHATE
TRITOLYL PHOSPHATE
BIPHENYL
l,2-DIBROMO-3-CHLORO PROPANE
HEXACHLORO BUTADIENE
HEXACHLORO CYCLOPENTADIENE
2 , 2 ' , 4 ' , 5-TETRABROMO BIPHENYL
O-CYMENE
D-LIMONENE
D,L-ISOBORNEOL
1-INDANONE
2-INDANONE
BUTYLATED HYDROXYTOLUENE
COUMARIN
OCTAMETHYL-CYCLOTETRAS ILOXANE
ETHYL HYDROCINNAMATE
2 -METHOXY-3 -METHYLPYRAZ INE
2 , 2 ' , 4 , 4 ' , 5-PENTACHLORO
DIPHENYL ETHER
4-CHLORO-P-TERPHENYL
TRICHLORO-P-TERPHENYL
2-PHENYL PHENOL
0
0
0
4
2
0
0
0
0
0
80
96
0
0
0
18
0
72
2
0
0
0
0
24
115.
139.
137.
50.7
48.0
OTHER
9.68
11.7
12.0
10.3
12.4
17.7
11.7
11.3
11.2
10.7
11.3
10.7
17.8
57.3
50.5
5.97
40.8
62.3
24.0
57.7
69.4
68.5
30.4
24.3
4.84
5.83
5.98
5.16
6.22
21.0
264.
5.66
5.59
5.34
11.8
5.34
46.7
29.1
25.3
2.99
20.4
31.1
93.7
<51.9
<62.5
<61.7
<22.5
<21.6
<4.83
<5.82
<5.97
<5.15
<6.21
<6.10
<6.12
<5.65
<5.58
<5.33
<5.56
<5.34
<6.75
<25.8
<22.8
<2.69
<18.4
<28.1
<10.8
53.5
64.5
63.5
23.5
22.4
3.21
3.86
3.96
3.42
4.12
18.4
246.
3.75
3.71
3.54
5.97
3.54
27.9
26.8
23.5
2.77
18.9
28.9
12.7
330.
398.
392.
276.
138.
31.7
38.2
39.2
33.8
40.8
93.2
785.
37.0
36.6
35.0
166.
35.0
312.
164.
145.
17.1
117.
179.
1820.
-------
Characterizing the Distribution of NHATS FY86 Semivolatile Compound
Concentrations (in ng/g, Unadjusted for Surrogate Recoveries) Based on All 50 Composite Samples
(cont.)
Compound Number
and Name
Percent
Detected
Avg.
LOD
Avg.
Cone.
Minimum
Cone.®
Median
Cone.
Maximum
Cone.
PESTICIDES (QUALITATIVE)
M
85 ISOPHORONE
86 DICHLOROVOS
98 CHLORPYRIFOS
99 ISOPROPALIN
100 BUTACHLOR
101 NITROFEN
102 PERTHANE
106 DICOFOL
107 P.P'-METHOXYCHLOR
88 2,4,6-TRICHLOROANISOLE
89 2,4,6-TRICHLOROPHENOL
90 2,4,5-TRICHLOROPHENOL
91 2,3,6-TRICHLOROANISOLE
92 2,3,6-TRICHLOROPHENOL
9 5 PENTACHLOROANISOLE
96 PENTACHLORONITROBENZENE
97 2,3,4-TRICHLOROANISOLE
110 OCTACHLORONAPHTHALENE
105 BENZO (A) ANTHRACENE
108 BENZO (B) FLUORANTHENE
109 BENZO (K) FLUORANTHENE
111 DIBENZO (A,H) ANTHRACENE
79 1-NONENE
80 CUMENE
16
2
28
10
12
8
0
6
0
5.00
5.00
5.00
10.0
5.00
5.00
10.0
5.00
10.0
5.50
3.65
7.00
5.50
9.60
16.1
5.00
11.2
5.00
CHLORINATED AROMATICS (QUALITATIVE)0'
0
0
0
0
0
2
0
4
2
PAHs
26
10
4
0
OTHER
50
34
10.0
10.0
10.0
10.0
10.0
10.0
5.00
10.0
10.0
(QUALITATIVE)0'
5.00
5.00
5.00
5.00
(QUALITATIVE)0'
20.0
5.00
5.00
5.00
5.00
5.00
5.00
5.10
2.50
10.0
5.30
4.45
3.79
8.60
2.50
112.
11.9
<5.00
<5.00
<5.00
<10.0
<5.00
<5.00
<10.0
<5.00
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<10.0
<5.00
<10.0
<10.0
2.50
2.50
2.50
5.00
2.50
2.
5.
50
.00
2.50
5.00
100.
60.0
40.0
10.0
200.
300.
5.00
300.
5.00
5.00
5.00
5.00
5.00
5.00
5.00
2.50
5.00
5.00
5.00
5.00
5.00
5.00
5.00
10.0
2.50
200.
20.0
4.45
3.79
8.60
2.50
<5.00
<5.00
<5.00
<5.00
2.50
2.50
2.50
2.50
10.0
30.0
300.
2.50
<20.0
<5.00
15.0
2.50
800.
200.
-------
Characterizing the Distribution of NHATS FY86 Semivolatile Compound
Concentrations (in ng/g, Unadjusted for Surrogate Recoveries) Based on All 50 Composite Samples (cont.)
Compound Number
and Name
Percent
Detected
Avg.
LOD
Avg.
Cone.
Minimum
Cone.®
Median
Cone.
Maximum
Cone.
OTHER (QUALITATIVE)®' (cont.)
81
82
83
84
87
93
94
103
104
1,2, 4-TRIMETHYLBENZENE
HEXYL ACETATE
1 , 3-DIETHYLBENZENE
1 , 4-DIETHYLBENZENE
QUINOLINE
DIBENZOFURAN
CHLORDANE
CHLOROBENZYLATE
BIS (2-ETHYLHEXYL) AD I PATE
62
82
8
0
8
0
2
0
10
5.00
5.00
10.0
10.0
10.0
20.0
10.0
10.0
9.89
39.5
132.
6.20
5.00
15.6
10.0
6.90
5.00
11.9
<5.00
<5.00
<10.0
<10.0
<10.0
<20.0
<10.0
<10.0
<5.00
25.0
85.0
5.00
5.00
5.00
10.0
5.00
5.00
5.00
200.
800.
20.0
5.00
400.
10.0
100.
5.00
100.
(1) Concentrations expressed in ng/g. Concentrations for not detected results are replaced by one-half of
^ the detection limit (LOD) prior to calculating statistics. Data for all 50 composite samples are included
w in the statistics for all compounds.
C) "<" indicates the minimum reported concentration was at the indicated detection limit.
&* Qualitative compounds were only monitored for detection versus non-detection.
-------
APPENDIX F
Estimates of Average Concentrations with 95% Confidence Intervals
As Determined by the Additive Model,
for Selected Subpopulations in the FY86 NHATS
-------
Codes used on the horizontal axes in the Appendix F plots:
Census region
NC = North Central
NE = North East
S = South
W = West
Race
W = White
NW = Nonwhite
Sex
M = Male
F = Female
F-l
-------
I
to
6000-
5000-
no
§ 4000
-4J
C!
o
£ 3000
v
00
CO
4>
J 2000-
"eo
6
1000-
0-
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=p,p-DDE
I I
NC NE
l^
S
I 1 I I
0-14 15-44 45+
I I
W NYT
I
M
I
F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=p,p-DDT
500-
400-
'oo
U)
o
v>
a
£ 300-
c
0)
u
e
0
o
V
BO
CO
« SOO-
TS
'
/
/
//
^
/
^
r
>
/
•
/'
•'
/
f
e
)
l
NC NE S W 0-14 15-44 45+ 1
i
/
/
f
/
/
/
1
f
i
i
i
• i
i
i
i
i
f
*\
T-
•p
^9C
i 1
i m M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=Beta-BHC
400-
5 300-
oo
^C^
c
.2
2
(3
u
"c
03
S
i 100-
u
0-
)
i
f
^ N
;
^
^ —
v
4
/*>
*\
)
f
\
\
\
\
\
\
)
i
/
/
/
/
)
_ •
xi
s
X
<"
;
/
/
/
/
^
/ -U
i
i
i
1 X
/ *
j*
?
/
/
l'
^
/
/
f
/
P
T-
^ ^^
\
)
\ f
/^
/
X
X
/
/
/
f
1 1 1 1 1 1 1 I 1 1 1 1 1 1 1 1
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=Heptachlor epoxide
100-
90-
t3 80-
£
1 7°~
2
-*j
•2
8 6°-
7 3
01 &
(rt ~
u
V
^
•*
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound-Oxychlordane
180-
170 :
160 :
150 :
'
^140:
c°
^ 13°-
o
? 120-
u
£ 110-
7 | 100 J
°* « :
« 90 :
u
>
< 80-
•& •
*> *?r>
o
& :
•3 RO
W "
50 :
40-
30 :
20:
)
i
f
^
)
{.---*
)
(
\
i
^
X
X
X
X
^
• •
3
(
i
i
/
i
i
i
"*
)
i
i
i
i
/
(
(
i
i
i
i
i
i
i
i
i
i
i
i
(
t
cv
X
X
x)
J
\
X
S
^
J-
i i ii i i i i i i r
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound-Trans-nonachlor
300-
§ aoo-
u
"c
V
o
o
0
Q)
«g
u
3
| 100-
(0
S
0-
3
i
i
//
£
3
/
!
/
j
e >
3
^
\
\
\
\
N
\
\
3
W
p /
/
^
^
)
^
/'
/
f "
i
f
i
i
t
5
^
1 1 1
f 3
•r
H
\
\
\ T
\
\
(
\
\
\
x \
h
J-
i l
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=Dieldrin (Corrected)
09
c
o
c
a>
u
a
u
a>
•o
0)
*>
a
B
w
Ed
110-
100-
90-
80-
70-
60-
50-
40-
30-
20-
10-
0-
)
«
t
f
t
\
\
•\
\
\
\
\
S
)
•
/
"^)
)
t
/
f
3
i i
\
\
\
\
\
\
\
^
\
3
U^
-->
)
f
,)
s
f
X
g
, •
)
--"*
f
II II I l l
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound^ 1,4-Dichlorobenzene
300-
1 2°° '
03
"e
0)
0
7 §
1 0
*° w
00
•3
"S 100
*J
CO
»»
CO
Ed
0-
\
1
3
/
/
X
X
X
X
v
;
• -
)
f
/
t
p
X
\
\
\
\
\
\
\
\
X
X
X
X
X
X
X
S
1
3
^
f
x
\
X
\
X
X
\
/
^
1 1
1
/
/
f
\
)
^
V
1
NC NE S W 0-14 15-44 45+ V
\
,
i
i
i
i
i
i
i
i
i
i
i
^ m
f
"1-
"
K
N
X
\
N
X
V
f %
l |
IT NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
H
O
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound«Hexachlorobenzene
110-
100-
-5 9°:
1 80
'•3
(0
c
8 7°-
c
o
0
0)
w> 60 -
S? •
£
1> 50-
"a
M
*^
H 40 -
30-
20-
)C
-L
)
1 l
)
/
/
t'
/
•
\
\
\
\
\
\
\
\
\
)
m
*
t
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
£
1 J.
/
/
f
'f
)
/
/
/
/
( ^
1
)
t
1
1
t
1
1
1
f
1
)
^
1 1
(-^
^5
•t-
f
\
X
1 1 l l 1
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=Naphthalene
40-
x: so-
I
i
s
1
J 20
Q>
00
a
v
0
E
10
^
6-
i
NC
I
NE
W
0-14 15-44 45+
I
W
I
NW
M
I
F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=Tetrachlorobiphenyl
130-
120-
110-
,
'So 100-
QO
C
— 90-
e
0
"g 80-
«*J
c
V
e 70-
t_« O
7 u
H « 60 -
N 0
|^
V
5 50-
tJ
V
•g 40-
6
2 30-
20-
10-
0-
)
I
r )
(
1
)
X
X
f
s
r
f
\
\
\
^
\
\
\
\
\
\
\
\
f
\
\
S
S
\
S
/
)
f
t
)
f
/
{
1
\
1
I
f
1
1 .
I
:
i
i
i
i
i
*
'
/
i
i
f
j
)
\
j
)
i
tt
/
f
I
T
}*
1
/
'
/
/
)C
1 1 1 1
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound-Pentachlorobiphenyl
300-
'oo
1 2°°"
"a
"c
u
o
e
o
f ^
V
W)
(,
«
^
J 100
ea
s
2
£
0
4 *
)
i
X
?
f
>
/
/
f'
f
^
/ /
* j
* /
' 1
\ '
i *
\
V
X
J. X
X
X
X
".
_.
—
/
V
\
N
\
'»
S
1 1
)
f
\.
}
f
f
f
*
/
1
1
1
)
f
1
'
r
f
1 1
*
£ - *"
' *
)(
/
\ /
f
/
\ '
J-
1 1
NC NE S W 0-14 15-44 45+ W N¥ M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
I
M
•*».
s
c
o>
o
C
4)
00
s
V
(0
6
2
CO
ta
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound«=Hexachlorobiphenyl
600-
500-
•
•
400-
300-
200-
100-
0-
)
l
f
)
1
/
/
/
/
/
/
f
P /
/
f
;
\
%
\
\
\
\
\ -i
\
\
/ \
/
/ i
f
I
f
•>.
"^
•+.
K
")
C
3
I
*
/
/
i
i
i -I
/
/
/
/
/
/
/
/
/
/
/
/
i
j
)
/
/
/
/
/ .
i
/
/
i
. i
i
i
i
i
i
»
t
3
I
5
/
/
/
/
/
/
/
/
g
i
f
i
i
t
(
\t
+ \
X
X
"'' 1
1
1 1 1 1 1
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
«
H
Ul
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound«Heptachlorobiphenyl
400-
$3oo-
c
c
o
"0
"c
4)
O
C
£ 200-
a>
00
0
1*
V
•<
•e
"0
6
"S 100 ~
0-
3
i
:
/
/
C
3
»
• 1
1
1
1
f
t
1
1
1
i *
\
\
\
\
\
\
\
\
\
\
\
L \
3
f
-•-
(x
V
""5
(
3
1 1
}
/
•
/
/
/
*
f
/ *-
i
i
i
i
i
C 3
l 1
i
/
/
/
/
/
/
/
/
/
/
f
" *
(
K
\
s
1
"
•«-
i 1
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=0ctachlorobiphenyl
140-
130-
120-
^ no:
00 ;
c :
•2 90 :
•v* OO ~
0>
03
S 40 -
"w
u 30-
20-
10-
0-
^
)
.
/
)
i
i
i
t
i
i
i
i
i
t
i
i
i
i
i
i
t
t
\
\ T
\
«
\
\
\
\
\
\
\
\
\
\
\
\
3
( )
3
1
/
t
w
)
1
,)
*>
(""
i
i
i
i
i
i
i
i
i
t
>
;
i
i
' )
/
r
f
r /
/
'
/*
.
•
i
9
f
\
)
f
\
\
\
\
\
\
f
l l I ill
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=Total PCBs
1300-
1200-
1100-
^55 •
bo 1000 -
3- '
e
.0 900 -
ta
t*
c 800-
0)
o
fi
£ 700-
0)
£ 600-
>
^£
•o 500
4>
"3
| 400
CO
W
300
200
100
)
1
;
1
)
/
/
/
/
I
. -
/
'
'
'
f
t
f
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
\
«
J
^
N
\
\
\
\
S>
/
)
1
NC NE S W 0-
)
/
f
/
/
/
/
/
/
f
)
/
I .
i
i
i
i
i
i
i
i
i
i
i
i
• i
i
i
f
1
f
f
)
1
V
i
/
/
/
/
/
/
/
/
\
"
_if
; -" T
' )f '
f
L- J-
1 1
14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
Total PCBs are the sum of estimated concentrations for Tetra- through Octa-CB.
-------
Estimated Level of Chlorination (%) with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
100-
90-
80-
70-
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound= 1 —Nonene
500-
400-
c
.2
2 300-
e
o
e
_, o
*fl o
1
.li «
E S?
u
« 200-
^^
•o
V
1
63 100
0
x
f
/
/
i
/
!
/
(
c
\
\
\
\
\
\
\
\
\
^
3
f
N
N
S
V)
)
f
}
/
r
f
\
\
\
\
\
N
\
)
II ll
)
f
1
>
/
/
r
r
/
i
\
)
f
\
X
X
X
X
X
>
1
f
1
NC NE S W 0-14 15-44 45-f W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
Estimates of Average Concentrations with 95% Confidence Intervals as Determined
by the Additive Model for Selected Subpopulations in the FY86 NHATS
Compound=Hexyl Acetate
400-
5j300-
c
o
"rt
u
"c
0)
o
7 £ 200-
o °>
0 W)
(0
V
^
^J
T3
"
(0
i i°o-
t3
0
)
i
S
L )
\
/
f
/
j
X
X
X
^*
{
f
\
\
\
\
\
\
\
\
V
\
\
\
\
3
N
f
/
S
^
t "
^
x)
^ ^
#• ^
S
N
\
7
II 1 1
3
/
/
/
f
y
f'
/
/
t
/
*
)(
^
X
>'''
^
\ 1 1
NC NE S W 0-14 15-44 45+ W NW M F
Nation
Census Region
Age(yrs)
Race
Sex
-------
APPENDIX 6
Concentrations (ng/g) from the FY82/ FY84, and FY86 NHATS,
Plotted in Chronological Order
with Age Group as the Plotting Symbol
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS.
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=p,p-DDT
1500-
:
1400-
1300^
1200-
1100-
^ 1000 -
bo
ja 900-
3,
0 §800-
1 23
H 2 700-
d
o 600-
c
5 500 '
400-
300^
200-
100-
0-
2
1
i 1
2 3
3
2 3
tfi 2 1 l 12 1 1
I1 31 32 333 ia 3 23!
2
3
31 3 33 2
. O2 o ** *» Qo
O 1 <6 ^> *< O
M f. O Ol O • • ***& ^ O IM ^> *3
«^(j » f\ £ Ci O3 1 9 6 y^ O
« XI
2
3 3
33 3 3
3
3
3 3
3
3 2 3
« _ 3 1 3tl 2 23 J
22 22 22^3 3^
221 ! j ! 3 1 2 1
13 3 2 i23 |
1
i
•
FY82
FY84
FY86
Plotting Ssrmbols: 111 0-14 years 222 15~44 years 333 45+years
Not-detected concentrations are expressed as LOD/2. Concentrations NOT adjusted for surrogate recoveries.
-------
O
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=p,p-DDE
12000 -
11000-
10000 -
9000-
^ 8000-
3 7000 -
c
3 6000 -
(0
u
§ 5000 -
o
e
0
0 4000 -
3000-
2000-
1000-
0-
1
3
2
2g 33
3 3 l
,,J8 3 3 22 3
3jl ^ 1 3 3 ,
^* M t *% * 1 jfc ^J
. < X y I ^^^
11 1Z 33
3
3
2 2 2S •*» o 3
ft o_ 1 22 <2 3
' «i» P *^l o2 3 ^^ o 2 fo o
^1 21 1 Jll 1
3
3
3
3 3 3
2
3
3
3
3
3 2
J 3
333 3
3o -a 2
S»J 3 2 o !
* 3 0 2 2 2
2 9 3
88 1 21 1 2
i 1 3
1 1 1
1
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS.
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Beta-BHC
1000-
•
900-
800-
•
700-
"M
oo 600 -
>B ;
o '
0 3 500 -
1 £
w i
c
o 400-
c
o
o
300-
200-
100-
0-
1
2 3
3
2
2
1
2
3
3 3
3
3 3
1 3
3 3
3
2 2 3 3 2
o p 3 p ° •;
Ol ^ ^ 1 '
2 o *
, 2 P
3 1 1 i 2
I1
1 1 1
3
3
3
1 1
j2 3 2 3 j
2 23 22 2
1 1 IP 3 3 q
3 2 2 2 p o
1 1 2?
3
3
3 3
tj
3 3
1 3 3
3 1
3 ! q
22 ^
*? 2 3 3
k , 3 31 3 2
23 3 23 1
n r
2 222 f
'i,1 i '3 s
21 1
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
O
Concentrations (ng/g) from the FY82, FY84, and FYB8 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound-Heptnchlor epoxide
400-
300-
00
3
7 '
3 20°-
E
«•>
g
0
c
o
0
100-
0-
1
2
2
3
3
3 o 3
# 3 o3 3 3
™ ,
«
-------
vn
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound-Oxychlordane
400-
300-
g
a 200-
1 •
8 :
c
o
o
100-
0-
•
3
3 3 2
3 3
3 22^ 3 2 33
2 2233, _
2 3 3^2 ^ 2 2
3 33 2 2 1 22 1 1 «
2 23 1 1 i 1 U
3
3
33 2 3 3 2 3
23 3 1 e33
3 2333 J
3
2 2
2 3 22
2
> ' 13
2 2131 312 ! 1
i
r
FY82
FY84
FY88
Plotting Symbols: 111 0-14 years 222 15~44 ye*" 333 45+years
Not-detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Trans - nonachlor
700-
600-
500-
"3>
^
3 400-
e
o
0 3
1 ts
o* £
g 300-
0
o
o
200-
100-
0-
2
2
3
3
3
3 3 22
23 3' 3 3 ,2 I
1 2 i o o
^ 21 3123g3 1 12T 1 3^3
3
hf 3 ^ , 3^ ,»
o lo Q 3<2 _ 2
S 2^3°22*3
2 * 1 1
3
3
3 3
3 2
333
3 o 3
o •» Co
3 3 3 3 3 3
2 2 3 %3 \
2 3 o 1
2 32
3 2i 1 i 2
2 1
112 2
>
FY82
FY84
FY86
Plotting Symbols: 111 0~ 14 years 222 15—44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82. FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Dieldrin
1200-
1100-
•
1000-
900-
^ 800-
00 :
J? 700-
C !
3 600 -
-------
o
1300-
1200-
1100-
1000-
900-
800-
J3 600-
c
0)
c 500^
o
u
400 4
300-
200-
100-
0-
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Hexachlorobenzene
\
\
t V
3ii2
FY82
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Mot—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Naphthalene
110-
100-
90-
80-
^ 70-
&
JB,
^ 60-
0 S
I T*
10 is 50-
c
o
o 40-
30-:
20-
10-
0-
1
2 3 X
2 3
3
1 3
3 !3 2 3
1 1 3 2 3
231 2 22 3333! !223 32 1 3
2
2 1
1 2 3
2 2 J 3,2
S3 333 2^13! 3 2 ^ &&Z&&& 3 3
1
3
3
1 1
2 3
v.v.1 3^32
3 2 q 2 i3 3 3 i
3 2 3 2 J
2 1 332 3 1
3
1
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45-f years
Not-detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Tetrachlorobiphenyls
400-
•
300-
W)
c
o
'•§ 20° -
u
"c
o>
u
e
o
o
100-
0-
3
2 oS3 « 3 32
2 1 2 ^3 2 ,
2 _ 1 . 2 3t3 o 3 2 12
13 21 3!2323 1 31 l 1T8 1 3 J
, 3 ^^
3
33 2 2 2
23 2
2 2 223i323 23
^ 1 1 1 1 2gl 1 31 3 21 12 2
3
3
3
3 3
3
3
3
o 3
3 „
o 33
32 3
,2
U 3 , 3
2 2
3
*» O **
3^3 ^
E2 2 2 lV« 2 1
1> 1 , 1
1 1 1 2 112 j
|
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 !5-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound* Pentachlorobiphenyls
700-
600-
500-
,-*
^
3 400-
G
o
o 3
i S
£ g 300-
o
c
cS
200-
100-
0-
1
3
2
3 3
3 3
3 3 o.
3 2 23 2
™ r» *5
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS.
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound- Hexachlorobiphenyls
1500-
1400 -
1300-
1200-
1100-
^ 1000
'^w^
y 900-
c
0 | 800-
M £ 700-
•I
5 600-
c
0 500
400-
300
200-
100-
0-
1 1
3
2 3
3
3
3 3
223 '3 # 3 2
2 12 z 3 -
2i 1 1 1 ^p „.
13 1 1 312323 311 3 '
3
2
2 2
33 3 j> 3 3 n 3
3 3 3 3
2 3 223222 3222 Z *&*
i 1 i 2 <
» l , 1 1 2 l 1 i
1 \i 1 *
3
3 3 3
3
9 3 3 3
2 3
93
2 3 2
3 2 g3 3 3
,3 3 2 ^ '.
2 2 3 J
2*? « n
91 2
1 3«
^
1 1 1
11 11
1
P
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82. FY84, and FY86 NHATS.
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound^Heptachlorobiphenyls
1200-
'
1100-
1000-
900-
^ 80O-
J? 700-
3 600-
| 500-
e
0 400
3OO-
200
100-
0-
1 3
q 3*-
1 o 3 33
\J
l>fa 13 113131321 CO2;
3
2
3 2 3 ^
2L „ « «3 2 „ 1
^jo *j ^^O **o«3
o o ^ 2 ^ 2r2 o *2
5 3 1 1 1 ! 2 1 i u 2! ! 2
3
3
3
3 3 3
3
2 2 3 3 3 3
22 3
/ ^3 3 %, 2 ^/a
2111 1 1 1 lrf#l, ^
1
>
FT82
FY84
FY86
Plotting Symbols: 111 0-143rears 223 15~44y«*rs 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=0ctachlorobiphenyls
500-
400-
^300-
Concentration (
N
o
o
100-
0-
i
3
3
3
2
3i 3 3 23
3 , l3 3
* ,223
221 1 21 % 2l 3 13 13231 2 & Z
3
2 3
3 3 2
feS^BtetelStf 222l3l 112322323 2123 122323
3
3
3 3
3 3 3
% 1
3
32 3
3 2 3 2 3
21 1 3o 3 o I
2 21 13312 1 l 1 33 2^112 J 2? 3 23S
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
o
t-»
Ul
5000-1
4000-
3000-
o
'•S
£
*j
c
S 2000
o
u
1000
#131
Concentrations (ng/g) from the FY82. FYS4, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Di-n-Butyl Phthalate
13 2
3
3' a. %2I
FY82
|23S1313
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
O
Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Butyl Benzyl Phthalate
3000-
^ 2000 -
oa
o
• *•«
"i->
U,
^j
C
o
e
o
0 1000-
0 -
1
31
2
2
33 *23
3 13 1
2 1 3 2
31 2322 3 5
|2rl31 12 23 !3 1 2 23 33
f
2 21!
«_ T_ 1 »»
23V33121 3
,4, 'a.3i2
1(^1 -rv— X ^n ff\ 4J 11 i?!n I Q *-» !?K5
23T13l33 2 ^3 322 3^3 33 " *<332333322r^
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45+years
Not—detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
Concentrations (ng/g) from the FY82, FYS4, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Bis (2-Ethylhexyl) Phthalate
30000 -
20000 -
Q
<30
a
o
•3
t
o
c
o
10000 -
0-
23Z3331212131
FY82
FY84
12 2
3 133281313 3332331123
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45+years
Not-detected concentrations are expressed as LOD/2. Concentrations are NOT adjusted for surrogate recoveries.
-------
APPENDIX H
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84,
and FY86 NHATS, Plotted in Chronological Order
with Age Group as the Plotting Symbol
-------
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=p,p-DDT
1300-
1200 :
1100-
1000-
'So
BO 900-
3.
g 800-
0
•o 700-
-j
.2. 600-
^
1
^ 500 :
a '.
oa
2 400-
co
300-
200^
100-
0-
2
.
1
,
3
3
2 3
3 3 3 9
3 3 2
2
! i2 2 i l i
i ii i2 1
1 3!32 333 3 235
.
2
3
3
^3 2- %3
1
-------
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=p,p-DDE
12000 -
11000-
10000 -
•
^ 9000 -
00
3 8000-
6
e
g 7000 -
* •§ 6000 -
10 .2.
*f 5000 -
3
g> 4000-
a
w 3000 -
2000-
1000-
0-
3
2
\ 3 3
3 1
3 3 2 „
w ^_ o
-_ O ^
rt O
2 22 ' :3 3 3 i *
1 1 2 1 2
11 1Z 33
3
3
o 33
2 2 23 3
f2 1 2 22 2 2 3
3 2 31 # 31 , 2 2 12 2
1 21 1 I1 1
3
3
3
3 3 3
2
3
3
3 3
-_ ^
3 3
3J3 3 3 3 «
3^ 3 322 £
23 2 o
1
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Beta-BHC
1000-
900-
800-
^_^
60
^ 700-
d
g 600-
o
•o
•g 500-
•*-•»
1 40°-
"«
§?
fc 300-
W
200-
100-
•
0-
1
2 3
3
2
1
2
3
3 3
3
3 3
1 3
3 3
3
**/ tl 32} '«.'
1
1 J l l
3
3
— i
3
1 *
2
2 l
2 3
3 2 3
23 2 *
1 3! ' t %' "" 3 %
22 3 iJ22
1 1 2*
3
3
3 3
3 3
' 3 • ',.'' %
* .V 3^
% 3 "3 ^3
2 8 &•
2 1 l ,3 Z
'l 2' 1
!
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45+years
Not-detected concentrations are expressed as LOD/2.
-------
Surrogate-Adjusted Concentrations (ng/g) from the FYB2, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound** Heptachlor epoxide
600-
•
500-
3 400^
d
c :
o
0
•e
•§ 300-
•r?
1
0)
»» \
g»200-
|
OT
100-
0-
2
2
2
3
3
3 3 \
p2 s3 3 3
1 3 1 2 3 2
^ 21 3^ 23 1 J 1 3
3
3
3 3
3
2 3 2
23 o i
~ « 2 23 2 2 3
O OM 2
' « 1 3 22 2 2
32 J 2 1 t
3-33 2 J i
2^ 1 121 1 1 1
3
3
3 3
3 3 23 3 3 3 2 ^ 3
3 3 1 2 3 *33 3 #8 «1
232 i 2 i 1 1 ^
1 2 1
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 lg~44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
Ul
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound" Oxychlordane
400-
^ 300-
00
•£
6
C
O
o
•o
1 200-
<
» ;
a
bO
o
w 100-
•
•
•
•
0-
3
3 2
3 3
3 3 n 3
2 3
2ff <&3L»
^3 9
2 3 3 2 Z2
22
33322 1 22l ! 12
2E3 in 1U
3
3
2 ^
33 33
33 2 3 3 2 3
23
3 2 3 3 ! 3 S
2 3 2
,3
2
1 ! 13
2 2131 312 ! j
•
FY82
FY84
FT86
Plotting Symbols: 111 0-14 years 222 lg~44 years 333 45+years
Not-detected concentrations are expressed as LOD/2.
-------
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Trans - nonachlor
900-
•
800-
700-
3 600-
o
c
o
S 50°-
•o
a 5
1 CO
<* 3
is" 4oo-
<
i
_2
(0
g»300-
t*
3
CO
200-
100-
0-
2
2
2
3
3
3
3 3 22
*3 r 3 3 12 .
1 2 t J 3
J3 21 312323 1 12 1 33
3
«3 3
% 332 33 23
S^ 2^3 2«»
_ 2 J
1^1 22 2 122
1 1
3
3
3 3
3 2
332U
3 3 3 3 33 23 ^
2 2 q 23 j
2 o 3 3,2 1
W « ,2lll3 H *
1 1 2 2 j
r
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
Surrogate—Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound-Dieldrin
1200-
1100-
1000-
^ 900-
tjfl ;
J? 800-
o 700-
•o
0)
•g 600-
•f 500-
§ 400-
w 300-
200-
100-
0-
2
3
3
3
s3
2 3
^1 J 2
1
1 3 J
SsV 2l% 2% 3 I3 1 312 2312 ^ !
»
1
2
1
)
«
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 ! 5-44 years 333 45+years
Not-detected concentrations are expressed as LOD/2.
-------
3000 -I
3. 2000 -
a
i
do
3
CO
I
**
g> 1000
|
w
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Hexachlorobenzene
I I
13H21
22
a
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
Surrogate—Adjusted Concentrations (ng/g) from the FY82. FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Naphthalene
120-
110-
100-
^ 90-
oo ;
J? 80-
6
c
o 70-
•o
0)
w 60-
•2. :
•f 50^
la
00 40 -
2 ;
a
w 30-
20-
10-
0-
1
2
1
2 1
2 3
3
3 ,3 2 3
2 !
2
2 1
1 2 3
2 2 322
pl g O 3 1 < 41
231 22 333l^33 J 2fe333322l3l3233 3323233|2 ^ 33
1
1
3
3
i
1 1
% 3 ,
32° I o z
6 q 3
31
3!2 122 30 31!2 3 '
3 3 222
213323
\
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45+years
Not-detected concentrations are expressed as LOD/2.
-------
M
O
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Tetrachlorobiphenyls
300-
•
1
3 200-
6
c
o
0
0)
w
a
I :
i
9)
§> 100-
to
0-
3
3
o *^^ "^
^ q
O O
2 1 2 3 2
Q O 1
21 2 1 232
13 21 g^ 1 31 l 1 2 1 3 j
3
3 3'
3
3
2 2
33 2
23 2
**
2 22 _ 2
2 3 1 3 3 2 3
233 2 2
k 111 221 1 31 3 21 12 2
3
3
,
, 3 3
3
3
3
o 3
3
3 B 2
3 ,
33 2
3
3 2 %3 ^
2l1 i ' i i w \
|
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
Surrogate—Adjusted Concentrations (ng/g) from the FY82. FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound-Pentachlorobiphenyls
s
M
M
600-
500-
J? 400-
d ;
o
o
•e
0)
•£ 300-
•5"
i
•s
a> 200-
§
CO
100-
0'
-
3
2
3
3
3
3 3
83 2
2 2
3 , 3
2 J o 3>
2 3 -2
2, 3
1 3 3213 1 % J
2l 21 ^ , 1 1
2
3
3 3
3 2
q 3 3
3 3
3 ,22
2 _ 3 3
3 2 2 92
3 2 22 2
• •
i I1 211 32 2 2
1 131 11
3
3
3
3
3 3
3 3
3 ^
1 V 2
3 2
1 22
3 2J3 3, „ 9t
** 1 Ob
1X3 3
3 22 3 2 2
22u i2 x 3' i
'
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not-detected concentrations are expressed as LOD/2.
-------
H
to
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Hexachlorobiphenyls
1200-
1100-
1000-
^ 900-
^
3 800-
o
c :
o 700 -
o
•o
400-
w 300-
200-
100^
0-
1
3
3
2
3
3
3
3
13 2
2 2
2' 3 * 2
12 3 1
2 ! 1 1 2g
% l3^ 311
3
2
2
« 3 3 o
30 n «3
O «J
C 0
3 3 3 3 o
•^ 2 0 2 3
3 22 222 22 2 32
2 3" 2 2
' V1 2l\ i J
3
A
3 3 3
3
*S j.
3 3
3 3 ffl
2 2
3 2 23 3 3
3 3 o 2 3 2
2 2« z
& 3 o
2 1 a/' ^
2, 1 l lt3
1 1 1
;
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
Surrogate—Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Heptachlorobiphenyls
a
1
H
W
900-
800-
700-
3 600-
6
a
o
£ 500-
•o
v
1
;«• 400-
i ;
"a
g» 300-
OT
200-
100-
0-
3
3
3 ^
3 2
3
2 * 3
« C q
! ." 32
2, X 1 13 2
2 31 21 3 1 I3 122 ! 123 J
3
2
3 23
2 3
3 P
33 23 3 2 3 a 33
3 2 222 ^ 32
2 3 *2 2
^ 1111 21U1 1 1
3
3
3 3 3
3 Q
2 2 3 3 3 3
22 3
3 3 3 2Q 3 3
2 32 l %2 3
211 1 1 1 I1 # li ^
^
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15"~44 years 333 45+ years
Not-detected concentrations are expressed as LOD/2.
-------
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=0ctachlorobiphenyls
400-
^ 300-
1
o
c
o
0
•g 200-
*f
Surrogate-^
h-
O
0
0-
3
3
3
2
31 3 3 23
3 13 3
13 l I2 2 3
1O« ?1
«
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
Ul
5000
4000-
g 3000
o>
CO
I 2000
cm
o
CO
1000-
0-
#131
Surrogate—Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Di-n-Butyl Phthalate
I
I
21
231
43 v«
w O "
[2321313
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45+years
Not-detected concentrations are expressed as LOD/2.
-------
Surrogate-Adjusted Concentrations (ng/g) from the FY82, FY84, and FY86 NHATS,
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Butyl Benzyl Phthalate
3000-
00
3 2000 -
6
c
o
o
1 "O
H £
<* »
1
1000 -
u
t.
w
0 -
1
1
1
3
2
2
3 3 ^
3 13 1
2 3
1 2
0 31 2322 3 !
|2*131 12 23 13 1 2 23 33
' 2 2ll
OQ ^"Vkl^^l *^
_ 33t*l*3 « *i^ i /^^
23r^3l33 g ~3g ^^ j22^3^3 33 *^3 %32Q33322<^
1
1
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 !5-44 years 333 45+years
Not—detected concentrations are expressed as LOD/2.
-------
X
I
Surrogate-Adjusted Concentrations (ng/g) from the FY82. FY84, and FY86 NHATS.
Plotted in Chronological Order with Age Group as the Plotting Symbol
Compound=Bis (2-Ethylhexyl) Phthalate
30000 AI
I
I
•S
3 20000
ci
c
a
T>
u
I
2P 10000 -
eo
0-
12383331212131
12 2
12321313 23s 32 133221313 333333112333233332222$
FY82
FY84
FY86
Plotting Symbols: 111 0-14 years 222 15~44 years 333 45-f years
Not-detected concentrations are expressed as LOD/2.
-------
APPENDIX I
Arithmetic Averages (and Standard Errors) of Extractable Lipid
Concentrations (ng/g) for Compounds Analyzed in the FY86 NHATS
and Also Analyzed in the FY82 and/or FY84 NHATS
-------
Table 1-1. Arithmetic Averages (and Standard Errors) of Extractable Lipid Concentrations (ng/g.
Unadjusted for Surrogate Recoveries) for Compounds Analyzed in the FY86 MEATS
and Also Analyzed in the PY82 and/or FY84 NHATS(1)
FY82
FY84
FY86
Compound
p, p-DDT
o , p-DDT
p,p-DDE
o,p-DDE
o,p-DDD
ALPHA-BHC
BETA-BHC
6AMMA-BHC ( LINDANE )
DELTA-BHC
ALDRIN
DIELDRIN^
ENDRIN®
TRANS-NONACHLOR
OXYCHLORDANE
HEPTACHLOR EPOXIDE
HEPTACHLOR
MIREX
GAMMA-CHLORDANE
1 , 2-DICHLOROBENZENE
1,2, 3-TRICHLOROBENZENE
1,2, 4-TRICHLOROBENZENE
1,3, 5-TRICHLOROBENZENE
1,2,3, 4-TETRACHLOROBENZENE
1,2,3, 5-TETRACHLOROBENZENE
1,2,4, 5-TETRACHLOROBENZENE
PENTACHLOROBENZENE
HEXACHLOROBENZENE
Mean
111.
1070.
175.
105.
76.0
44.7
10.0
10.1
7.07
6.58
68.4
(Std. Error)
PESTICIDES
( 23. )
( 170. )
{ 24. )
( 20. )
( 17.3 )
( 9-1 )
( 1-42)
CHLOROBENZENES
( 1-6 )
( 0.52)
( 0.37)
( 30.7 )
Mean (Std.
90.0 (
6.73 (
817. (
7.15 (
62.3 (
9.96 (
134. (
9.45 (
9.08 (
6.55 (
25.5 (
19.4 (
75.0 (
47.3 (
49.1 (
9.54 (
7.40 (
6.52 (
6.52 (
7.31 (
6.52 (
6.52 (
6.52 (
6.52 (
6.52 (
24.3 (
Error)
12.4 )
0.25)
82. )
0.47)
14.8 )
3.43)
18. )
2.56)
1.91)
0.17)
8.6 )
3.8 )
7.0 )
5.0 )
5.9 )
1.46)
0.69)
0.17)
0.17)
0.57)
0.17)
0.17)
0.17)
0.17)
0.17)
3.4 )
Mean (Std.
227. (
5.46 (
3010. (
2950. (
6.87 (
6.75 (
5.50 (
209. (
8.74 (
6.15 (
5.79 (
70.0 (
54.3 (
72.8 (
161. (
123. (
81.3 (
17.6 (
12.1 (
5.41 (
5.14 (
5.88 (
5.08 (
5.53 (
5.84 (
5.79 (
5.38 (
5.04 (
54.7 (
Error )
37. )
0.71)
360. )
420. )C)
0.89)
0.87)
0.71)
20. )
2.45)
0.80)
0.74)
7.7 )
8.3 )<4>
8.0 )
17. )
12. )
6.6 )
11.9 )
1.7 )
0.70)
0.66)
0.76)
0.66)
0.72)
0.76)
0.75)
0.70)
0.65)
5.2 )
-------
Table 1-1. (cont.)
FY82
FY84
FY86
Compound
Mean (Std. Error)
Mean (Std. Error) Mean (Std. Error)
PHTHALATE ESTERS0)
DIMETHYL PHTHALATE
DIETHYL PHTHALATE
DI-N-BUTYL PHTHALATE
BUTYL BENZYL PHTHALATE
BIS (2-ETHYLHEXYL) PHTHALATE
76
348
246
.3
.
.
( 27.
( 112.
( 59.
PHOSPHATE
TRI BUTYL PHOSPHATE
TRIPHENYL PHOSPHATE
TRIS (2-CHLOROETHYL) PHOSPHATE
TRITOLYL PHOSPHATE
33
1840
29
.4
.
.6
( 2.
(1730.
( 4.
5 )
)
)
TRIESTERS
5 )
)
3 )
7
7
207
57
19
(3)
7
65
19
24
.10
.64
•
.4
.4
.10
.8
.4
.3
( o
( o
( 44
( 17
( 3
( o
( 48
( 3
( 3
.44)
.64)
. )
.5 )
.8 )
.44)
.4 )
.8 )
.8 )
13.
17.
63.
58.
1010.
57.
30.
69.
24.
6
9
0
0
7
4
4
3
( 1.5 )
( 2.7 )
( 16.5 )
( 7.4 )
( 560. )
( 6.3 )
( 5.7 )
( 7.6 )
( 2.6 )
PAHs
NAPHTHALENE
PHENANTHRENE
FLUORANTHENE
CHRYSENE
ACENAPHTHENE
ACENAPHTHALENE
FLUORENE
PYRENE
14
8
6
.4
.23
.63
( 2.
( 0.
( o.
0 )
73)
38)
9
20
7
10
6
6
8
20
.47
.5
.18
.3
.52
.57
.29
.0
( o
( 7
( o
( 1
( o
( o
( 1
( 11
.89)
•7 )
.44)
-7 )
.17)
.18)
.40)
.6 )
20.
5.
5.
5.
5.
5.
6.
5.
5
92
44
61
36
51
09
11
( 2.5 )
( 0.73)
( 0.69)
( 0.71)
( 0.69)
( 0.71)
( 0.79)
( 0.66)
PCBs
MONOCHLOROBIPHENYLS
D ICHLOROBIPHENYLS
TRICHLOROBIPHENYLS
TETRACHLOROBIPHENYLS
PENTACHLOROBIPHENYLS
HEXACHLOROBIPHENYLS
KEPT ACHLOROB I PHEN YLS
9
21
69
123
62
.46
.4
.7
.
.8
( 0.
( 2.
( 9-
( 19.
( 11.
95)
8 )
7 )
)
2 )
6
6
10
34
77
135
93
.52
.52
.8
.0
.3
.
.5
( o
.17)
( 0.17)
( o
( 4
( 10
( 14
( 14
.8 )
•7 )
•1 )
• )
.0 )
6.
6.
16.
88.
188.
422.
176.
41
49
5
1
( 1.05)
( 1.06)
( 2.1 )
( 10.7 )
( 21. )
( 42. )
( 27. )
-------
Table 1-1. (cont.)
FY82
FY84
FY86
Compound
Mean (Std. Error)
Mean (Std. Error)
Mean (Std. Error)
PCBs (cont.)
OCTACHLOROBIPHENYLS
NONACHLOROB I PHENYLS
DECACHLOROB I PHENYL
46.0
22.7
39.1
( 11.2 )
( 6-8 )
( 4.1 )
12.7
14.4
16.5
( 2.9 )
( 2.2 )
( 2.3 )
60.7
25.7
32.6
( 11.1 )
( 4.1 )
( 4.3 )
H
I
U)
(1) For samples having not-detected results, the measured concentration is taken to be one-half of the LOD.
Refer to Table 8-6 to determine how often' this substitution is made. Statistics are presented only for
those compounds analyzed within a given survey.
® Quantiation ion used: m/z=316.
0) Results based on only 13 samples in FY84.
(4) Corrected data (see Section 5.1.2).
-------
Table 1-2. Arithmetic Averages (and Standard Errors) of Extractable Lipid Concentrations (ng/g,
Adjusted for Surrogate Recoveries) for Compounds Analyzed in the FY86 NHATS
and Also Analyzed in the FY82 and/or FY84 NHATS(1>
FY82
FY84
FY86
Compound
Mean (Std,
. Error )
Mean (Std. Error)
Mean (Std. Error)
PESTICIDES
p,p-DDT
o,p-DDT
p,p-DDE
o , p-DDE
o , p-DDD
ALPHA-BHC
BETA-BHC
GAMMA-BHC ( LINDANE )
DELTA-BHC
ALDRIN
DIELDRIN^
ENDRIN0)
TRANS-NONACHLOR
OXYCHLORDANE
HEPTACHLOR E POX IDE
HEPTACHLOR
MIREX
GAMMA-CHLORDANE
193. (
1850. (
303. (
182. (
132. (
77.5 (
17.3 (
38. )
280. )
39. )
34. )
29. )
15.0 )
2.3 )
136.
10.1
1230.
10.8
93.9
15.0
201.
14.2
13.7
9.87
38.5
29.2
113.
71.3
74.1
14.4
11.2
9.82
( 18. )
( 0.4 )
( 120. )
( 0.7 )
( 21.3 )
( 4.9 )
( 26. )
( 3.7 )
( 2.8 )
( 0.24)
( 12.4 )
( 5.5 )
( 10. )
( 7.2 )
( 8.6 )
( 2.1 )
( i.o )
( 0.24)
200.
4.79
2650.
2590.
6.03
5.93
4.83
184.
9.01
5.40
5.08
61.5
47.7
64.0
141.
108.
63.7
15.5
10.6
4.75
( 31. )
( 0.58)
( 300. )
( 350. )®
( 0.73)
( 0.71)
( 0.58)
( 16. )
( 2.30)
( 0.65)
( 0.61)
( 6.3 )
( 6.8 )<4>
( 6.5 )
( 14. )
( 10. )
( 4.7 )
( 9.7 )
( 1.4 )
( 0.57)
CHLOROBENZENES
1 , 2-DICHLOROBENZENE
1,2, 3-TRICHLOROBENZENE
1,2, 4-TRICHLOROBENZENE
1,3, 5-TRICHLOROBENZENE
1,2,3, 4-TETRACHLOROBENZENE
1,2,3, 5-TETRACHLOROBENZENE
1,2,4, 5-TETRACHLOROBENZENE
PENTACHLOROBENZENE
HEXACHLOROBENZENE
19.9 (
13.9 (
12.9 (
118. (
3.1 )
0.9 )
0.7 )
52. )
22.4
25.1
22.4
14.8
14.8
14.8
15.1
42.9
( 0.5 )
( L7 )
( 0.5 )
( 0.3 )
( 0.3 )
( 0.3 )
( 0.4 )
( 5.9 )
6.77
9.48
8.19
8.92
7.62
7.56
7.02
6.65
55.1
( 0.80)
( 1-12)
( 0.96)
( 1.05)
( 0.92)
( 0.91)
( 0.84)
( 0.80)
( 4.9 )
-------
Table 1-2. (cont.)
FY82
FY84
FY86
Compound
Mean (Std. Error)
Mean (Std. Error) Mean (Std. Error)
H
I
01
DIMETHYL PHTHALATE
DIETHYL PHTHALATE
DI-N-BUTYL PHTHALATE
BUTYL BENZYL PHTHALATE
BIS (2-ETHYLHEXYL) PHTHALATE
132.
604.
427.
PHTHALATE ESTERS(3)
(43. )
( 153. )
(
63. )
PHOSPHATE TRIESTERS
TRIBUTYL PHOSPHATE
TRIPHENYL PHOSPHATE
TRIS (2-CHLOROETHYL) PHOSPHATE
TRITOLYL PHOSPHATE
NAPHTHALENE
PHENANTHRENE
FLUORANTHENE
CHRYSENE
ACENAPHTHENE
ACENAPHTHALENE
FLUORENE
PYRENE
MONOCHLOROBIPHENYLS
DICHLOROBIPHENYLS
TRICHLOROBIPHENYLS
TETRACHLOROB I PHENYLS
PENTACHLOROB I PHENYLS
HEXACHLOROB I PHENYLS
HEPTACHLOROBIPHENYLS
57.
3190.
51.
24.
14.
11.
15.
31.
137.
242.
123.
9 (
4.2 )
(2870. )
4 (
6 (
0 (
3 (
6 (
5 (
(
(
(
7.1 )
PAHs
3.4 )
1.2 )
0.6 )
PCBs
1.5 )
4.0 )
18. )
37. )
21. )
14.3
12.1
462.
141.
39.1
(3)
10.7
99.1
29.2
36.7
14.6
31.6
11.0
15.8
10.0
10.1
12.8
30.7
9.91
10.1
16.8
52.7
120.
208.
145.
( 0.7 )
( 0.9 )
( 77. )
( 26. )
( 6.3 )
( 0.6 )
( 69.7 )
( 5.5 )
( 5.5 )
( 1-3 )
( 11-6 )
( 0.7 )
( 2.6 )
( 0.2 )
( 0.3 )
( 2.1 )
( 17-5 )
( 0.24)
( 0.2 )
( 1-2 )
( 7.0 )
( 15. )
( 20. )
( 21. )
13.1
17.2
60.8
55.9
975.
55.6
29.3
67.0
23.5
20.3
5.87
5.39
5.56
5.31
5.46
6.04
5.06
6.25
5.84
14.8
70.1
157.
351.
146.
( 1.3 )
( 2.4 )
< 14.9 )
( 6.7 )
( 500. )
( 5.7 )
( 5.1 )
( 6.9 )
( 2.4 )
( 2.4 )
( 0.70)
( 0.67)
( 0.68)
( 0.67)
( 0.69)
( 0.76)
( 0.64)
( 0.97)
( 0.87)
( L7 )
( 7.9 )
( 16. )
( 32. )
( 20. )
-------
Table 1-2. (cont.)
H
I
ON
FY82
FY84
FY86
Compound
Mean (Std. Error)
Mean (Std. Error) Mean (Std. Error)
OCTACHLOROBIPHENYLS
NONACHLOROBIPHENYLS
DECACHLOROBIPHENYL
92
37
62
.6
.3
.3
PCBs
( 21
( 10
( 5
(cont.
•7 )
.8 )
•9 )
)
19.
22.
25.
7
3
7
( 4
( 3
( 3
.3 )
•3 )
.3 )
51.9
23.1
31.1
( 8
( 3
( 3
.5 )
•4 )
•5 )
(1) For samples having not-detected results, the measured concentration is taken to be one-half of the LOD.
Refer to Table 8-6 to determine how often this substitution is made. Statistics are presented only for
those compounds analyzed within a given survey.
surrogate recoveries.
® Quantiation ion used: m/z=316.
(3) Results based on only 13 samples in FY84.
W Corrected data (see Section 5.1.2).
See Section 5.2 on the method for adjusting data for
-------
APPENDIX J
Comparisons of Predicted Average Concentrations (ng/g) by
Selected Subpopulations for Selected Semivolatiles
over the FY82, FY84, and FY86 NHATS
-------
Table J-l. Comparisons of Predicted Average Concentrations (ng/g) by Census Region for Selected
Scmri vn1»M 1 aa nvar- t-ha WVR2 . WVBA anri PVR£ KTHaTest1)
Semivolatiles over the FY82, FY84, and FY86 NHATS
i
H
FY82
Compound
p,p-DDT
p.p-DDE®
BETA-BHC
TRANS -NONACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
TETRACHLOROBIPHENYL
Census
Region
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
Mean (S.E.)
44.0
244.
298.
133.
1030.
1960.
2520.
1610.
159.
366.
434.
138.
36.8
264.
97.8
50.6
30.4
146.
44.7
26.1
27.4
440.
27.0
35.4
18.3
13.5
15.1
15.7
(19.4)
(62.)
(62.)
(60.)
(400.)
(710.)
(630.)
(960.)
(62.)
(118.)
(105.)
(116.)
(15.3)
(108.)
(34.5)
(46.7)
(9.9)
(53.)
(12.5)
(20.0)
(15.3)
(309.)
(14.2)
(38.5)
(2.6)
(2.0)
(1.8)
(4.3)
FY84®
Mean (S.E.)
98.2
111.
164.
101.
940.
1510.
1070.
1150.
171.
216.
179.
254.
87.0
108.
128.
84.5
75.2
57.1
80.5
50.1
41.8
33.0
29.0
80.1
54.4
51.6
46.7
41.5
(12.2)
(23.)
(18.)
(25.)
(95.)
(240.)
(100.)
(240.)
(29.)
(62.)
(29.)
(83.)
(5.9)
(11.)
(8.)
(10.2)
(10.7)
(11.1)
(10.7)
(11.3)
(6.2)
(7.8)
(4.1)
(24.3)
(8.2)
(11.8)
(7.0)
(11.6)
FY86
Mean (S.E.)
136.
273.
132.
202.
1820.
2310.
2240.
3240.
151.
157.
177.
130.
89.2
156.
154.
116.
63.5
48.4
70.5
37.7
41.2
57.6
41.7
74.7
66.2
78.8
46.9
34.0
(24.)
(57.)
(23.)
(51.)
(310.)
(490.)
(360.)
(940.)
(43.)
(55.)
(43.)
(55.)
(26.2)
(33.)
(26.)
(34.)
(7.4)
(9.1)
(7.3)
(9.4)
(5.4)
(8.8)
(5.5)
(13.6)
(8.6)
(11.6)
(7.9)
(10.6)
FY86-FY82
Diff .
91.7
28.9
-167.
69.3
787.
351.
-280.
1630.
-8.21
-209.
-257.
-8.48
52.4
-109.
56.7
65.1
33.1
-97.4
25.8
11.6
13.8
-382.
14.7
39.2
48.0
65.3
31.8
18.2
(S.E.)
(30.7)
(83.7)
(66.)
(78.2)
(505.)
(861.)
(723.)
(1340.)
(75.4)
(130.)
(114.)
(128)
(30.3)
(113.)
(43.3)
(57.7)
(12.4)
(54.1)
(14.5)
(22.1)
(16.2)
(309.)
(15.2)
(40.8)
(9.0)
(11.8)
(8.1)
(11.4)
FY86-FY84
Diff.
37.5
162.
-32.6
101.
881.
795.
1180.
2090.
-19.8
-58.8
-2.05
-124.
2.20
48.1
26.7
31.2
-11.7
-8.72
-10.0
-12.4
-0.587
24.6
12.7
-5.41
11.8
27.2
0.169
-7.53
(S.E.)
(26.7)
(61.)
(29.4)
(56.)
(321.)
(545.)
(370.)
(970.)
(51.5)
(82.3)
(51.4)
(100.)
(26.8)
(35.1)
(27.4)
(35.3)
(13.0)
(14.4)
(13.0)
(14.7)
(8.235)
(11.7)
(6.9)
(27.9)
(11.9)
(16.6)
(10.54)
(15.7)
-------
Table J-l. (cont.)
FY82
Compound
PENTACHLOROBIPHENYL
HEXACHLOROBIPHENYL
HEPTACHLOROBIPHENYL
TOTAL PCBS(4)
CHLOR. LEVEL (%)(5)
Census
Region
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
NC
NE
South
West
Mean (S.E.)
63.2
76.1
92.6
76.6
125.
147.
260.
132.
76.7
24.1
86.3
161.
328.
295.
508.
464.
59.3
58.4
59.2
60.3
(9.2)
(12.3)
(11.6)
(22.0)
(43.)
(61.)
(48.)
(70.)
(25.0)
(32.9)
(23.3)
(60.)
(51.)
(71.)
(56.)
(99.)
(10.6)
(16.6)
( 7.6)
(14.5)
FY84®
Mean (S.E.)
94.1
178.
104.
88.9
172.
245.
211.
159.
113.
136.
142.
117.
448.
627.
524.
428.
57.9
57.8
58.4
58.4
(10.0)
(35.)
(10.)
(14.2)
(12.)
(28.)
(14.)
(17.)
(12.)
(23.)
(14.)
(20.)
(22.)
(52.)
(24.)
(33.)
( 3.2)
( 5.4)
( 3.0)
( 5.1)
FY86
Mean (S.E.)
165.
202.
107.
64.2
282.
430.
299.
250.
101.
213.
109.
85.5
648.
998.
595.
468.
57.7
58.5
58.4
58.8
(26.)
(34.)
(26.)
(33.9)
(30.)
(47.)
(30.)
(41.)
(38.)
(48.)
(38.)
(48.6)
(59.)
(80.)
(59.)
(77.)
( 6.2)
( 5.4)
( 6.8)
(11.5)
FY86-FY82
Diff.
102.
125.
14.5
-12.4
156.
283.
38.5
118.
24.5
189.
22.6
-75.6
321.
704.
86.7
4.0
-1.6
0.2
-0.8
-1.6
(S.E.)
(28.)
(36.)
(28.7)
(40.4)
(52.)
(77.)
(57.1)
(81.)
(45.2)
(58.)
(44.3)
(77.4)
(78.)
( 107)
(81.3)
( 125)
(12.2)
(17.5)
(10.2)
(18.5)
FY86-FY84
Diff.
71.4
23.3
2.77
-24.7
110.
185.
87.5
90.8
-12.1
77.3
-33.3
-31.7
201.
371.
71.5
39.9
-0.2
0.7
-0.0
0.4
(S.E.)
(28.1)
(48.8)
(28.3)
(36.8)
(32.)
(55.)
(33.1)
(44.2)
(39.6)
(53.1)
(40.1)
(52.7)
(63.)
(96.)
(63.5)
(83.9)
( 6.9)
( 7.7)
( 7.5)
(12.6)
Estimates originate from fitting the additive model on surrogate-adjusted concentrations.
Error due to MSA sampling is not included in the standard error estimates.
m/z = 316 in FY86 NHATS (see Section 5.1.2).
Sum of concentrations for tetra- to octa-chlorobiphenyl.
Overall chlorination level for PCBs, defined in Section 6.2.1.2.
-------
Table J-2. Comparisons of Predicted Average Concentrations (ng/g) by Age Group for Selected Semivolatiles
over the FY82, FY84, and FY86 NHATS(1)
oo
FY82
Compound
p,p-DDT
p,p-DT>E®
BETA-BHC
TRANS -NONACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
TETRACHLOROBIPHENYL
PENTACHLOROBIPHENYL
HEXACHLOROBIPHENYL
Age
(yrs)
0-14
15-44
45+
0-14
15-44
45+
0-14
15-44
45+
0-14
15-44
45+
0-14
15-44
45+
0-14
15-44
45+
0-14
15-44
45+
0-14
15-44
45+
0-14
15-44
45+
Mean
139.
206.
200.
1120.
1690.
2590.
129.
279.
429.
96.7
95.3
139.
43.9
51.4
82.6
100
100.
159.
14.2
12.2
22.0
40.5
68.3
121.
98.8
179.
229.
(S.E.)
(38.)
(41.)
(36.)
(370.)
(420.)
(630.)
(55.)
(68.)
(100.)
(31.4)
(29.6)
(39.)
(13.9)
(14.5)
(22.2)
(63.9)
(66.)
(82.)
(2.2)
(1.7)
(2.7)
(7.6)
(10.3)
(18.)
(30.9)
(34.)
(39.)
FY84®
Mean (S.E.)
64.6
121.
170.
558.
1170.
1540.
220.
170.
228.
47.1
94.4
162.
26.6
61.2
109.
28.7
42.8
53.5
14.8
46.7
76.8
38.8
117.
167.
63.8
215.
272.
(13.0)
(15.)
(20.)
(89.)
(120.)
(160.)
(48.)
(30.)
(37.)
(5.1)
(6.7)
(12.)
(6.1)
(9.5)
(17.)
(6.2)
(6.9)
(7.8)
(4.6)
(8.5)
(13.2)
(8.5)
(15.)
(20.)
(8.7)
(16.)
(21.)
FY86
Mean (S.E.)
73.0
177.
252.
1710.
2150.
3080.
100.
124.
247.
62.5
115.
203.
32.6
51.8
84.7
35.0
47.0
69.8
19.4
41.8
105.
75.6
107.
218.
101.
306.
481.
(26.6)
(29.)
(33.)
(380.)
(360.)
(410.)
(52.)
(41.)
(36.)
(32.1)
(25.)
(22.)
(7.6)
(6.1)
(5.5)
(6.6)
(5.8)
(6.5)
(9.0)
(7.4)
(8.)
(32.2)
(25.)
(22.)
(29.)
(30.)
(33.)
PY86-FY82
Diff .
-66.2
-28.8
52.5
589.
462.
485.
-28.9
-155.
-181.
-34.2
20.0
63.9
-11.2
0.373
2.07
-65.0
-53.1
-89.0
5.28
29.6
83.2
35.1
39.1
97.2
1.89
127.
252.
(S.E.)
(46.5)
(50.2)
(48.7)
(527.)
(555.)
(754.)
(76.2)
(79.)
(106.)
(44.9)
(38.8)
(45.2)
(15.8)
(15.72)
(22.9)
(64.2)
(66.1)
(82.4)
(9.26)
(7.6)
(8.7)
(33.1)
(27.2)
(28.3)
(42.5)
(45..)
(51.)
FY86-FY84
Diff.
8.43
56.3
81.9
1160.
978.
1540.
-120.
-45.3
19.3
15.4
20.9
40.9
5.99
-9.38
-24.7
6.22
4.17
16.3
4.66
-4.88
28.5
36.8
-9.84
51.9
37.0
90.8
209.
(S.E.)
(29.6)
(32.6)
(38.4)
(390.)
(381.)
(440.)
(71.)
(50.7)
(51.4)
(32.5)
(26.0)
(24.8)
(9.71)
(11.3)
(18.1)
(9.09)
(9.00)
(10.1)
(10.1)
(11-3)
(15.6)
(33.3)
(29.3)
(29.9)
(30.5)
(34.2)
(39.)
-------
Table J-2. (cont.)
FY82 FY84®
Compound
Age
(yrs) Mean (S.E.) Mean (S.E.)
HEPTACHLOROBIPHENYL 0-14 76.7
TOTAL PCBS(4)
CHLOR. LEVEL
(1)
(2)
(3)
(4)
(5)
Estimates
Error due
m/z = 316
15-44 84.0
45+ 91.1
0-14 285.
15-44 396.
45+ 511.
(%)(5) 0-14 60.1
15-44 59.6
45+ 58.7
originate from fitting
to MSA sampling is not
(20.0) 26.2 (8.8)
(18.8) 136
(18.3) 192
(40.) 158
(42.) 530
(47.) 731
( 9.4) 58
( 7.1) 58
( 6.2) 58
. (15.)
. (21.)
. (16.)
. (28.)
. (39.)
.1 ( 6.7)
.2 ( 3.5)
.0 ( 3.4)
the additive model on
included in
FY86
Mean
26.9
112.
217.
244.
596.
1100.
57.7
58.4
58.3
(S.E.)
(46.2)
(36.)
(32.)
(69.)
(57.)
(54.)
(19.2)
( 6.7)
( 3.3)
surrogate - ad j us ted
FY86-FY82
Diff.
-49.7
27.5
126.
-41.2
199.
590.
-2.4
-1.1
-0.4
(S.E.)
(50.3)
(40.
(37.
(79.
(71.)
(72.)
(21.
( 9.
( 7.
8)
)
2)
3)
8)
1)
FY86-FY84
Diff.
0.786
-24.4
24.7
86.1
65.1
370.
-0.4
0.2
0.3
(S.E.)
(47.02)
(39.1)
(38.0)
(70.4)
(63.7)
(66.)
(20.3)
( 7.5)
( 4.8)
concentrations .
the standard error estimates .
in FY86 NHATS (see Section 5.1.2).
Sum of concentrations for tetra-
to octa-chlorobiphenyl .
Overall chlorination level for PCBs, defined
in Section 6.2.1.
2.
-------
Table J-3. Comparisons of Predicted Average Concentrations (ng/g) by Race Group for Selected
Semivolatiles over the FY82, FY84, and FY86 NHATS(C
FY82
Compound
p,p-DDT
p,p-DDE0)
BETA-BHC
TRANS -NONACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
TETRACHLOROBIPHENYL
PENTACHLOROBIPHENYL
HEXACHLOROBIPHENYL
HEPTACHLOROBIPHENYL
Race
Group
White
NW
White
NW
White
NW
White
NW
White
NW
White
NW
White
NW
White
NW
White
NW
White
NW
Mean (S.E.)
150.
383.
1900 .
1520.
347.
15.1
120.
56.5
64.1
35.8
122.
102.
14.7
20.7
75.5
92.6
150.
307.
67.9
167.
(30.)
(163.)
(410.)
(1060.)
(66.)
(100)
(31.)
(43.2)
(14.6)
(18.5)
(71.)
(60.)
(1.5)
(4.5)
(8.9)
(28.0)
(30.)
(101.)
(17.4)
(44.)
FY84(2>
Mean (S.E.)
104.
220.
1200.
904.
203.
179.
105.
105.
68.2
68.7
42.8
43.6
49.6
44.8
115.
115.
190.
242.
119.
177.
(11.)
(48.)
(90.)
(170.)
(26.)
(53.)
(6.)
(14.)
(8.0)
(20.9)
(5.6)
(10.1)
(6.5)
(12.3)
(12.)
(20.)
(12.)
(32.)
(11.)
(33.)
FY86
Mean (S.E.)
152.
301.
2250.
2780.
146.
212.
130.
131.
58.8
51.6
51.9
48.2
53.0
73.0
133.
141.
289.
435.
111.
195.
(23.)
(75.)
(300.)
(690.)
(30.)
(69.)
(18.)
(42.)
(4.8)
(9.7)
(4.7)
(10.5)
(6.0)
(16.0)
(18.)
(42.)
(23.)
(65.)
(26.)
(61.)
FY86-FY82
Diff.
2.03
-82.0
343.
1260.
-202.
197.
10.6
74.2
-5.30
15.8
-69.6
-53.6
38.3
52.3
57.8
48.5
139.
129.
42.9
28.4
(S.E.)
(37.9)
(180)
(506.)
(1270.)
(72.)
(121.)
(36.3)
(60.4)
(15.3)
(20.9)
(70.7)
(60.6)
(6.2)
(16.6)
(20.5)
(50.7)
(38.)
(120.)
(31.6)
(75.0)
FY86-FY84
Diff.
47.7
81.5
1050.
1880.
-57.6
33.6
25.7
26.2
-9.34
-17.0
9.16
4.56
3.42
28.2
18.6
25.8
99.2
193.
-7.85
17.9
(S.E.)
(25.1)
(88.8)
(310.)
(710.)
(39.8)
(87.1)
(19.2)
(44.5)
(9.34)
(23.1)
(7.31)
(14.6)
(8.83)
(20.2)
(21.7)
(47.0)
(25.7)
(73.)
(28.6)
(69.1)
-------
Table J-3. (cont.)
FY82
Compound
TOTAL PCBS(4)
CHLOR. LEVEL
W Estimates
® Err-OT due
Race
Group
White
NW
(%)(5) White
NW
originate from
ttn MS A aaitml 3 nc
Mean (S.E.)
336.
753.
58.8
60.5
fitting
i n H not-.
(37.)
( 122)
( 7.4)
(11.0)
FY84(2)
Mean
487.
614.
57.
58.
the additive
inr1! iidp
>ri in t
(S.E.)
(21.)
(53.)
9 ( 2.8)
8 ( 5.8)
model on
•he strand?
FY86
Mean
623.
913.
58.2
58.7
(S.E.)
(42.)
( 105)
( 4.6)
( 7.9)
surrogate - ad j us ted
iTd ei-rr
>T est-.i mattes
PY86-FY82
Diff.
287.
160.
-0.6
-1.8
(S.E.)
(56.)
( 161)
( 8.7)
(13.5)
FY86-FY84
Diff.
137.
298.
0.2
-0.1
(S.E.)
(47.)
( 117)
( 5.4)
( 9.8)
concentrations .
(3)
(5)
m/z = 316 in FY86 NHATS (see Section 5.1.2).
Sum of concentrations for tetra- to octa-chlorobiphenyl.
Overall chlorination level for PCBs, defined in Section 6.2.1.2.
o\
-------
Table J-4. Comparisons of Predicted Average Concentrations (ng/g) by Sex Group for Selected
Semivolatiles over the FY82, FY84, and FY86 NHATS(1'
FY82
Compound
p,p-DDT
p,p-DDEp)
BETA-BHC
TRANS -NONACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
TETRACHLOROBIPHENYL
PENTACHLOROBIPHENYL
HEXACHLOROBIPHENYL
HEPTACHLOROBIPHENYL
Sex
Group
Male
Female
Male
Female
Male
Female
Male
Female
Male
Female
Male
Female
Male
Female
Male
Female
Male
Female
Male
Female
Mean (S.E.)
184.
194.
1830.
1850.
287.
295.
116.
103.
67.0
52.2
116.
120.
12.4
18.8
81.9
75.0
197.
157.
124.
47.4
(44.)
(55.)
(400.)
(430.)
(76.)
(93.)
(33.)
(37.)
(15.8)
(16.9)
(67.)
(70.)
(2.1)
(2.8)
(11.0)
(12.8)
(38.)
(41.)
(22.)
(20.8)
FY84®
Mean (S.E.)
100.
146.
1270.
1030.
185.
212.
121.
88.9
75.9
61.0
42.9
43.0
39.8
57.3
110.
119.
225.
173.
163.
95.9
(16.)
(19.)
(150.)
(140.)
(34.)
(37.)
(9.)
(7.8)
(13.5)
(12.0)
(7.5)
(7.4)
(9.4)
(11.6)
(17.)
(18.)
(21.)
(18.)
(20.)
(15.1)
FY86
Mean (S.E.)
172.
181.
2240.
2430.
133.
179.
160.
102.
59.9
55.5
52.3
50.4
40.7
71.2
115.
153.
294.
332.
148.
104.
(28.)
(28.)
(370.)
(360.)
(40.)
(36.)
(25.)
(22.)
(6.0)
(5.5)
(6.1)
(5.6)
(7.6)
(7.4)
(25.)
(22.)
(29.)
(28.)
(35.)
(32.)
FY86-FY82
Diff.
-12.1
-12.2
404.
586.
-154.
-116.
44.4
-0.552
-7.11
3.35
-63.8
-69.8
28.3
52.4
33.6
77.6
97.6
175.
23.9
56.1
(S.E.)
(52.1)
(61.6)
(541.)
(561.)
(86.)
(100.)
(40.9)
(43.47)
(16.9)
(17.7)
(67.7)
(70.3)
(7.8)
(7.9)
(27.1)
(25.6)
(47.8)
(49.)
(41.5)
(38.0)
FY86-FY84
Diff.
72.0
35.9
968.
1400.
-51.8
-33.2
39.3
13.1
-16.1
-5.49
9.42
7.40
0.887
13.9
4.95
33.8
68.9
159.
-15.3
7.64
(S.E.)
(31.9)
(33.5)
(399.)
(380.)
(52.7)
(51.5)
(26.4)
(23.5)
(14.8)
(13.1)
(9.67)
(9.31)
(12.10)
(13.7)
(30.1)
(28.4)
(36.0)
(33.)
(40.9)
(35.2)
-------
Table J-4. (cont.)
FY82
FY84g)
FY86
FY86-FY82
FY86-FY84
Sex
Compound Group Mean (S.E.) Mean (S.E.) Mean (S.E.) Diff. (S.E.) Diff. (S.E.)
TOTAL PCBS(4> Male 469. (46.) 557. (35.) 651. (56.) 181. (73.) 93.5 (66.2)
Female 347. (49.) 462. (32.) 692. (51.) 345. (71.) 231. (60.)
CHLOR. LEVEL (%)<*> Male 59.7 ( 6.7) 58.6 { 4.2) 58.9 ( 5.9) -0.8 ( 8.9)
(1)
(2)
(3)
(4)
(5)
Female 58.9 ( 9.5) 57.5 ( 4.4) 57.8 ( 5.0) -1.1 (10.8)
Estimates originate from fitting the additive model on surrogate-adjusted concentrations.
Error due to MSA sampling is not included in the standard error estimates.
m/z = 316 in FY86 NHATS (see Section S.I. 2) .
Sum of concentrations for tetra- to octa-chlorobiphenyl.
Overall chlorination level for PCBs, defined in Section 6.2.1.2.
0.3 ( 7.3)
0.3 ( 6.7)
C-l
i
00
-------
APPENDIX K
Plots of Estimates Average Concentrations (ng/g)
by Census Region and by Age Group,
Plus and Minus Two Standard Errors,
Based on the Additive Model
for the FY82, FY84, and FY86 NHATS
-------
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=p,p-DDT
500-
400-
c
o
2 300-
c
W
0
c
o
o
9)
00
O
£ 200-
ic
•o
"S
.§ •
»
W
100-
.
0-
)
1
•
)
I
1
i
)
1
3
i
i
t
i
i
i
i
i
i
i
i
i
)
S
/
f
f
/
k
f
\
1
1
\
\ -
\
'
\
\
1
\
\
\
\
\
\
\
\
:
i
i
i
i
i
(
f
)
1
^
t
)
t
/
f
f
\ _
\
X
\
)
f-
1
4
1
1
1
1
1
1
1
1
1
1
1
1
1
\
t
\
\
\
\
\
\
\
\ -,
\
\
1 \
1 \
S. j
)
/
f
(
f
1
FY82 FY84 FY86 NC NE S W NC NE S W NC NE ' S W
Nation
FY82
FY84
FY86
-------
10
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound-p.p-DDE
6000-
5000-
»*"s
**••*
g 4000-
'«
IM
"e
V
<3 3000-
**'
w
W
a
u
0)
3
3 2000-
(d
E
n
W
1000-
0-
T
)
)(
1
5K
»
3
^
/
/
/
t
i
i
i
/
r
)
/
f
f
X
/
f
t
\
\
\
*
\
\
\
3
~
{ )
.
f
•
C
S
N *p
^1 ^ "5
r .
3
(
_
;
X
f
f
t
f
C ~ — _5
4
/
/
/
/
/
/
/
/
/
f
i
I I T
FY82 FY84 FY86
I I I I I
NC NE S W
I i I I I I I I
NC NE S W NC NE S W
Nation
FY82
FY84
FY86
-------
I
u>
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Beta-BHC
700-
600-
'55
g> 500-
c
o
"a
I*
B 400-
W
o
e
o
o
0>
oo
£ 300-
§> '
fit
^*« .
•o
0)
"o
6 200-
_i_»
CO
W
100-
0-
K
3
1
/ "
)
3,
'
t
i
i
$ )
/
/
i
i
i
i
t
i
i
i
»
)
S
f
f
f
f
\
1
*
\ -.
*
\
\
\
t
\
\
\
\
\
\
\
\
\
\
\
3
5
x
1 1
_
S
X
X
f
>
•x
J
3
/
.'
/
/
\
_
^
T
*• ""*' *
N/ -if** %SX
X
1
-L
i i
FY82 FY84 FY86 NC NE S W NC NE S W NC -NE S W
Nation
FY82
FY84
FY86
-------
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Trans-nonachlor
500-
400-
GO
c
o
2 300
c
u
o
o
0)
00
(0
g! 200
•o
0)
w
100
)
)
« i J
f
)
S
i
1
1
1
1
1
1
1
1
'
1
1
1
1
1
1
1
1
1
1
1
'l
'
/
V
\
\
\
\
\ __
\
\
I -p
\
\ -p
\ 3^ "^c
IT T / ^
\ T ^)K^ / SN
v ^- " -^ Nv x7 '*
}> ^
\
L )( 1
C I -L
1 1 II 1 1 1 1 1 1 1 1 1 II
FY82 FY84 FY86 NC NE S W NC NE S W NC NE S W
Nation
FY82
FY84
FY86
-------
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound»Heptachlor epoxide
Ul
300-
1
g
5 200-
o
1
a
8
a
3
V
1
J>
^(
3 100-
cd
fl
,s
*3
a
0-
)
•
•
•
J
j
•
»
i
•
3
I
!
•i
/
(
/
/
i
/
/
i
i
! T
f *
)
1 1
;
/
»
(
1
\
<
1
\
1
\
( T
1 -p
\
\
\ \ t
V S f X \ T
1 s /ST 31
it '* ?( >
' * \
f "s JL IK,
m f
1 1 1 1 1 1 1 1 1 1 1 I f
FY82 FY84 FY86 NC NE S W NC NE S W NC NE S W
Nation
FY82
FY84
FY88
-------
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Hexachlorobenzene
1
c
o
IS
t.
"e
0)
o
c
o
0
V
9
I*
«
<
V
a
.1
w
W
1100-
1000-
900-
800-
700-
600-
500-
400-
300-
200-
100-
0-
i
i
;
i
/
i
/
i
T 1
1
1
1
1
1
1
^ /
i
1
5K X T
1 I j
f
i
t
i
\
i
i
t
\
\
\
\
\
i
i
i
1 T T
1 H 3K
X ^j §^ JD x-'^l S " " **" ~ - -J- * *"
I I
i i i i i i I I I 1 I I I I i i I i i
FY82 FY84 FY86 NC NE S W NC NE S W NC NE S W
Nation
FY82
FY84
FY86
-------
*
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Tetrachlorobiphenyl
110-
100-
90-
"w 80-
<**_0i'
c
-2 70-
£ :
"S
8 eo :
c
o
0
S, 50-
«J
(H
u
^ 40-
v [
a
CO
w ;
20-
10-
0-
V
;
T
1 1
)
S
^
X
)
1
(^ T
^-f *
1 1
)
^ ^
^ x
^")
f
\
)
/
"•)
)
/
'
/
/
\
\
\
\
\
\
\ T
\
\
\
\
\
\
\
i
t
\
\
\
3
1 1
FY82 FY84 FY86 NC NE S W NC NE S W NC NE S W
Nation
FY82
FY84
FY86
-------
X
I
00
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Pentachlorobiphenyl
300 4
3
c 200
o
fi
^>
G
U
u
e
V
bO
g
V
v 100
0)
g
W
Ed
)
\
3
•
f
)
/
(
)
„->
\
>
X
X
t'
f
^,
""«•
"•)
>
(
>
*
/
'
'
'
'
/
*
'
*
/
f
\
\
\
\
\
X
\
X
X
\
X "
X
X
/ s
/ '
f
f
•**
^ **\
;
)
V
/
t
/
f
f
\
\
\
\
\
\
\
\
\
\
\
\
-
X
t
•*" \
)
f
i
f
{
\
\
\
\
\
\
\
-------
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound-Hexachlorobiphenyl
)
)
T
^c
^S
I
f A
»
/ \
/ \
/ \
' \ —
t
_,
_
5
%
„ t
3
.
.
/
/
/
/
/
/
/
/ \
i \ _
/ \
/ \
\* • x
ff. X
\
\
\
\
%
\
\
\
\
< »
; \
• X
Nv
/ \
X
fx v X
/ )(^
/ ^
/ \
H N 1
' ^
^^
( 1
III 1 111
FY82 FY84 FY86 NC NE S W NC NE S W NC NE S W
600-
500-
>
g 400
c
V
a
a
300-
o>
S?
tn
S
5 200-
I
n
100-
0-
Nation
FY82
FY84
FY86
-------
Plot of Estimated Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Heptachlorobiphenyl
400-
60
C
.2
"as
"c
v
C
* (S 200-
H» Q,
O GO
CO
t*
>
•5
4)
CO
e
•S 100-
w
0
)
I
>
*
f
( )
L 5
i
\
f
c
\
\
\
*
\
L 5
3
.'
/
*
i
/
f
}
. i
1
i
i
\
. •
f
3
i
^
,'
{ '
•^
t---*
V
f
V
X
^x
)t
1
1
1
1
(
\
3
/
i
i
i
»
i
!
f
\
\
\
\ *
\
\
\
\
\
\
\
\
\
i
*
.
f
\,
X
N
• •
1 l 1 1 1 1
FY82 FY84 FY86 NC NE S W NC NE S W NC NE S W
Nation
FY82
FY84
FY86
-------
1200-
1100-
1000-
900-
800-
e
o 700
c
3
& 600
2
$
< 500
•o
o>
4->
g 400
co
w
300-
200-
100-
Plot of Estimated.Average Concentrations (ng/g) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Total PCBs
5
5
i
*
1
t
f
)
)
_ /
• t
t
""•*)
/
///
f
/»
f \
! \
j -1- \
;' \
T '' \
4
"")
)< " \
/ NS. H
/ N T N
• ' \ ^
/ -L \( -1- s
/ > s
C I' s ^C
T s^f
1
FY82 FY84 FY86
Nation
NC NE
W
NC NE
W
FY82
FY84
NC NE S
FY86
W
Total PCBs are the sum of estimated concentrations for Tetra- through Octa-CB.
-------
Plot of Estimated Level of Chlorination (%) by Census Region,
Plus and Minus 2 Standard Errors, Based on the Additive Model
H
M
100-
1
1
90-
80-
£ 60-
•d
s.
1 5°'
40-
30
20
•
)
i
n
c .
)
•
'82 FY
•
. t
( )
•
•
'84 FY
•
t
, )
( '
«
•
i
86 N
•
/
C N
L - - -J
S
E i
m
3 1
C
)
•
i
V N
m
t J
•
C N
•
•
k
e — J
•
E i
•
/ &
r — ^
•
3 1
j
( )
•
i
V N
•
^
fr " "
C N
>
/ ^
r J
E £
/_ ^
f- — -s
i
S V
/
t
i
1
Nation
FY82
FY84
FY86
Level of Chlorination is the sum of the percentage of Total PCBs for each homolog
(Tetra- through Octa-CB), weighted by each homolog's chlorine mass fraction.
-------
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=p,p-DDT
400-
u»
W)
d
.2
"«j
t*
d
300-
200-
00
£
1
v
-------
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=p,p-DDE
4000-
3000 -
o
I
V
o
2000-
Q>
60
CO
OJ
03
«
1000-
0
)(
3J
K
I I I
FY82 FY84 FY86
I I I
0-14 15-44 45+
I I I
0-14 15-44 45+
I I I i
0-14 15-44 45+
Nation
FY82
FY84
FY86
-------
700-
600-
500
e
o
£
I O
M °
Ul Q)
t,
V
400-
300-
200-
01
Ed
100-
0-
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Be ta - BHC
FY82 FY84 FY86
Nation
—i 1 r~
0-14 15-44 45+
FY82
T
T
0-14 15-44 45+
FY84
—i 1 1 r
0-14 15-44 45+
FY86
-------
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Trans - nonachlor
300-
00
tjfl
c 200
o
g
-4-j
c
V
o
o
o
CD
tn
100
(0
6
'*3
CO
w
—I 1 T—
0-14 15-44 45+
FY84
—I 1 T~
0-14 15-44 45+
FY86
—I 1 1—
FY82 FY84 FY86
Nation
0-14 15-44 45+
FY82
-------
H
•J
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound-Heptachlor epoxlde
150-
140-
130-
120-
5°
? no-
««*
a
.§ 100-
C
^s '
d 90-
w
J 80-
U)
E 70-
§•
« 80-
3
1 50.
•3 '
1ft
(3
pH4 ^ A '
4>U m
30
20-
10.
1
«
3
•
•
%
)
C
t
•
f
t
•
3
•
i
•
(
•
V
1
•
1
K
^
0 *
- X
\
•
k
I
1
9
'
/
(
, •
3
•
3
/
/
/
/
/
/
/
/
/
/
(
•
)
i
i
i
i
i
i
i
i
i
r /
' J
/
i
i
i
»
c
•p
. .
j \
'
.
f
j
}(
T *
/
/
f
t *
'
. -*
"
x
i i
FY82 FY84 FY86
Nation
0-14 15-44 45+
FY82
0-14 15-44 45+
FY84
0-14 15-44 45+
FY88
-------
00
400-
c
o
I
"c
o>
o
c
W
300-
200-
u
§
a
6
tS
100-
0-
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Hexachlorobenzene
—1(
-i
I T I
FY82 FY84 FY86
Nation
i i i i
0-14 15-44 45+
FY83
0-14 15-44 45+
FY84
0-14 15-44 45+
FY86
-------
I
H
VO
00
130-
120-
110-
100-
^ 90-
c
o
• ^H
"as 80 -
a
0)
u
C
o
u
0)
DO
(H
V
50-
•o
V
« 40
6
13
w __
u 30
20-
10-
0-
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Tetrachlorobiphenyl
)C
)(
1 1 1 1—
FY82 FY84 FY86
Nation
)<
h-r
—i 1 r~
0-14 15-44 45+
FY82
T
T
0-14 15-44 45+
FY84
—i 1—;—r~
0-14 15-44 45+
FY86
-------
I
to
o
300-
200-
» 100
CO
w
W
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Pentachlorobiphenyl
1 1 1
FY82 FY84 FY86
Nation
—I 1 T~
0-14 15-44 45+
FY82
0-14 15-44 45+
FY84
—I , r-
0-14 15-44 45+
FY86
-------
to
600-
500-
QO
fi 400
o
• »H
4->
a
t-.
"c
V
300-
0)
DO
(0
0>
200-
co
6
CO
100-
0-
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compourid-Hexachlorobiphenyl
/
/
—I 1 1—
FY82 FY84 FY86
Nation
—I 1 T~
0-14 15-44 45+
FY82
—i 1 r~
0-14 15-44 45+
FY84
—I f r-
0-14 15-44 45+
FY86
-------
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Heptachlorobiphenyl
300-
i
to
200-
£
o
C
5
V
60
£
V
2 100
CO
W
I I I
FY82 FY84 FY86
I I I
0-14 15-44 45+
I I I
0-14 15-44 45+
I l l
0-14 15-44 45+
Nation
FY82
FY84
FY86
-------
Plot of Estimated Average Concentrations (ng/g) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
Compound=Total PCBs
1300-
1200-
1100-
oo
00
e
o
2
2
1000-
900-
800-
e
0)
o
* J 700
10 Q)
U> 00
£ 600
I
"g 500^1
"S
I 400
ta
W
300-
200-
100-
—i 1 r~
0-14 15-44 45+
FY82
—i 1 r~
0-14 15-44 45+
FY84
1 1 1 1—
FY82 FY84 FY86
Nation
0-14 15-44 45+
FY86-
Total PCBs are the sum of estimated concentrations for Tetra- through Octa-CB.
-------
Plot of Estimated Level of Chlorination (%) by Age Group,
Plus and Minus 2 Standard Errors, Based on the Additive Model
100-
90-
80-
ft)
70-
I 8
-------
50272-101
REPORT DOCUMENTATION
PAGE
l._ REPORT NO.
" EPA 747-R-94-001
4. Title and Subtitle
Semi volatile Organic Compounds in the General U.S. Population
NHATS FY86 Results - Volume II
7. Author(s)
3. Recipient's Accession No.
5. Report Date
8. Performing Organization Rept. No.
9. Performing Organization Name and Address
10. Project/Task/Work Unit No.
11. Contract(C) or Grant(G) No.
(0
(G)
12. Sponsoring Organization Name and Address
Chemical Management Division
Office of Pollution Prevention and Toxics
U.S. Environmental Protection Agency
Washington, DC 20460
13. Type of Report & Period Covered
14.
IS. Supplementary Notes
Khoan T. Dinh
Technical Programs Branch
16. Abstract (Limit: 200 words)
The Environmental Protection Agency's National Human Adipose Tissue Survey
(NHATS) was performed annually to quantify the levels of selected chemicals in
the adipose tissue of humans in the U.S. population. Specimens collected in
fiscal year 1986 were earmarked for an analysis to estimate national average
concentrations of 111 semivolatile compounds in adipose tissue, to identify
differences in average concentrations among subpopulations, and to compare
results with previous surveys in the NHATS. For 17 semivolatiles detected in
at least half of the 50 analytical samples, statistical modeling techniques
were conducted to address these objectives.
Among demographic effects on average concentration, the age group effect was
most often statistically significant, with higher concentrations associated
with higher ages. Among PCB homologs, the 45+ year age group had from 188% to
706% higher average concentrations than the 0-14 year age group, with similar
increases observed for pesticides. Geographic effects were only occasionally
significant, and no significant race or sex effects were observed.
Statistically significant increases in concentration (generally less than
100%) from the FY82 NHATS were observed for three PCB homologs, while
increases of 50% to 100% from the FY84 NHATS were significant for p,p-DDT and
p,p-DDE. Mixed findings were observed for other semivolatiles analyzed in all
three surveys.
17. Document Analysis a. Descriptors
b. Identifiers/Open-Ended Terms
c. COSATI Reid/Group
18. Availability Statement
NTIS
19. Security Class (This Report)
20. Security Class (This Page)
21. No. of Pages
22. Price
(Sw ANSI-Z39.18)
See Instructions on Reverse
OPTIONAL FORM 272 (4-77)
(Formerly NTIS-35)
Department of Commerce
------- |