-------
Figure A-9-8,
Effect of bed depth on carbon required to remove 90% of an
inlet SC>2 concentration of 2,000 ppm and the pressure drop
across carbon + plates
Ui
o
60
i
6
t
"5
5
a.
&
S
e
40
30
20
10
70
60
§
e
Outlet Add Loading:
Linear Gas Velocity:
Inlet 02 Concentration:
Inlet H£0 Concentration:
Temperature:
0.184 Ib. Acid/lb. Carbon
2 Ft./Sec.
0.046 Volume Fraction
0.13 Volume Fraction
200° F
40
30
£
o.
20o
12
16
20
24
28
32
36
10
40
Settled Bed Depth, inches
-------
Figure A-9-9
Effect of bed depth on carbon required to remove 9070 of an
inlet S0£ concentration of 2,000 ppm and the pressure drop
across carbon + plates
60
I
u
* 50
£
tx
&
o
_ 30
a
20
10
60
Si
50.2
t.
3
Outlet Acid Loading:
Linear Gas Velocity:
Inlet 02 Concentration:
Inlet HgO Concentration:
Temperature:
0.184 Ib. Acid/lb, Carbon
3 ft./sec.
0.046 Volume Fraction
0.13 Volume Fraction
200 °F
40
30
20?
10
12 16 20 24
Settled Bed Depth/Stage, inches
28
32
36
40
-------
Figure A-9-10
hO
Effect of bed depth on carbon required to remove 90% of an
inlet S02 concentration of 2,000 ppm and the pressure drop
across carbon + plates
Outlet Acid Loading:
Linear Gas Velocity:
Inlet Og Concentration:
Inlet H20 Concentration
Temperature:
0.184 Ib. Acid/lb. Carbon
4 Ft./Sec.
0.046 Volume Fraction
0.13 Volume Fraction
200°F
20
16 20 24
Settled Bed Depth/Stage, inches
-------
APPENDIX A-9-1
EFFECT OF CARBON BED DEPTH/STAGE ON THE TOTAL
CARBON BED DEPTH REQUIRED TO REMOVE 90% OF
AN INLET S02 CONCENTRATION OF 2000 PPM
Linear Gas Velocity,
ft. /sec . Run Number
2 Test-1
2 Test-27
2 Test-28
2 Test-29
2 Test-30
3 Test-3
3 Test-31
3 Test-32
3 Test-33
3 Test-34
4 Test-4
4 Test-5
4 Test-6
4 Test-7
4 Test-8
4 Test-9
4 Test-10
4 Test-11
153
-------
S02 SORBER DESIGN
RUN NUMBER TEST-1 DATE 7 27 71
TOTAL CARUON RATE = 25.320 LBS/HR
OUTLET'CARBCN "LOAD ING = 6YT8375 ' LOSi""AC I D /'LB CARBON
HEIGHT OF CARBON/STAGE = 2.45 INCHES
D I AME TER OF V ES SE L_ = 18_.0_I_NCHES^__^
CAR DON" USED""=" ~o>
TOTAL GAS FLOW RATE = 948'.. SCFH
INLET S02 CONCENTRATION^ _2..000* PP^
"INLET 'NCTCON'CENTRAYlON = .~ T'50". PP'M: ; ;. ,''"'}:;.*"!';"
INLET 02 VOLUME FRACTION = 0.0460 , .;; ::': ;;" .:' ; :
INLET H20 VOLUME FR AC T I 0_N_=___0. 1_300_ -^ ^ '- ' '/j'v v--::j.
UUTLET"SU2 CONCENTRATION "= """200 . "P"PM~ "~
TEMPERATURE = 200.0 DF.G. F
S62'~CON'CENfRATTUN "TcTO" LOAD ING'"*
STAGE PPM , .-.;:"::. LBS ACID/LB CARBON
1 : 2000.-:-;>-:v:.'':.:;l'-::-::Xr::^: -..'-0.1837
1723. 0.1553
0.1249
0.0933
3
A
5
C
7
1426.
1117.
807.
511.
252.
0.031?.
0.0047
0.23 200.0001 0.0
TOTAL CARBON REQUIRED = 17.71 INCHES
TOTAL STAGES REQUIRED ASSUMING 2.45 INCHES;CARSON/STAGE -:7.23
SPACE VELOCITY = 3637. 1/HR
PRESSURE DROP ACROSS CARBON .='. ', : 8.86 INCHES H20
PRESSURE DROP ACROSS PLATES, = :/ 4 .43;-INCHES H20
IUT_AL PRESSURE DROP ACROSS .STAGES =;; :p3»28 INCHES H2o;
154
-------
S02 SORBER DESIGN
RUN NUMBER
TESY-3 DATE 7 27 71
TOTAL CARBON RATE = 37. 98_0__L.BS/HR __ ______
"OUTLET CARBOKfTbAUTNG" "="0". 1837b LbS ACT07TB~CARB"ON~
HEIGHT CF CARBON/STAGE = I. 85 INCHES,
J31AMETER OF VESSEL = 18.0 INCHES _ ________ ____ _
CARBON l"US"ED"= ..... ~" ..... 6."
TOTAL GAS FLOW RATE = 14227. SCFH
INLET S02 CONCENTRATION = _ 200p_. PPM
" I N L E f N 0 " "CO N C EN T R A T 1 0 N ='" ~~~ ^"7l 5 : 0"."
INLET 02 VOLUME FRACT ION - 0.0460
INLET H20 VOLUME FRACTION = Q.I 300
OUT LET 'SU"2~CONC"EN"firAnON "=
"P P M"
___
"200. PPM
TEMPERATURE = 200.0 DEG. F
1- ;::: STAGE
2
3
4
':.-. "A1". iMv:1-:-' :'. 6 X
^^OV^TH
8
9
10
: 11
: I i
;.--: . 12
S02 CONCENTRATION
::: :,-- PPM
:iV; '"':^' '2000.
1858.
1711.
1558.
£'£' I"--- .124*f*^.:w
920.
761.
607.
" ' £A 1 :.:J!"'lv:::O
f O JL . : :,:.v.v:: ::,...
ACID LOADING
LBS ACID/LB CARBON
0.1837
0.1692
0.1541
0.1385
:^%;.a :J:!*v,::;.:-i.;:.;-":.. ' 0. 1225 ... -. v .. . : ;.f ::;::i ;:,,-..-t
w4pps.f/:,;:>. . .'. 0.1061 '". :-vi:::--:^: .^Sii^iJ,.-
'-:, ':: .:-. ''; *-.-' : :: .:" ;' '-:-::: ;.-: .. __ ,,.,..... - ..>-. . . .- ;
.:.;: . . : . . ; :.- : ;:.,: f\ f\ (i G A - .-...-., : * - - - -
.;; ' ' '/ -. -".-.' '-: - . -, \j v \) o ^y o -:' .-:. . . , ' ; : - ":;:-.-. :-, - :.- .-.'
0.0731
0.0568
0.0410
On ~j A i '.'' -
* UC-O 1 .. .-...,... :...;...:
K:§ff::m. ^M ":. o .0122 " ' ""' v-^*f^:^:'.. .
lii:;v;:i'^,;:;i^:;:::;'; ..; o . o . &&&:'£**<'' '
0.06
200.0001
0.0
TOTAL CARBON REQUIRED = 24.16 INCHES
TOTAL STAGES REQUIRED ASSUMING;;!.851.INCHE.S CARBON/STAGE =13.06
SPACE VELOCITY =
4000. 1/HR
PRESSURE""i3ROT"ACROSS CARBON = ;; 12.08 INCHES H20
PRESSURE DROP ACROSS PLATES =; 6.04 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = >;:v' 18.12 INCHES H20
155
-------
S02 SORBER DESIGN
RUN NUMBER
TEST-4
DATE 7 27 71
TOTAL CARBON RATE =__5^0_ IBS/HR
"6 U T L E r C A R B 0 N ~ 10AD'ING = "6". 18 375 GTS" ACID*
HfclGHT OF CARbON/STAGE = 1.65 INCHES
DIAMETER OF VESSEL - 18.0 INCHES
"CARBON
TOTAL
INLET
INLET
CARBOf
USED = 0.
GAS FLOW RATE = 18969. SCFH
S02 CCNCFNTRATION_=_ 2000. PPM
"NOCCNCENTRATTO'N =
INLET 02 VOLUME FRACTION =
INLET 1120 VOLUME FRACTICN =
OUTLET SO 2" CONCENTRATION "=
150.
0.0460
0.1300
PPM"
200". PPM'
TEMPJERATURE = 200 .0_ DEG._ F _
~'~S02~C'ONCE>yfRATION"
STAGE PPM
I -: 2000.
ACID LOADING
LBS ACID/LB CARBON
0.1837 ,
2
3
4
5
6
7
8
9
id
.::,.: ' n
14
15
16
; 17 .
i " 0.86
1905.
1807.
1706.
1604., -.:;
1285.
1176.
1067.
958:. v;
850^-vP*
744.- :::;>.
640.
539.
442.
351.
267.
200.0001
0.1740
0.1640
0.1537
'h^mMt'f&i.Q'1'*!*-
0.1105
0.0993
0.0881
^^m^:^--.:. '- 0.0770 , . . .:;. , . ', -: :,..;.-, . ... -:;,
!;::$l;1^IS?':-;i;.;^ 0.0659 '', ';' ' 1 ' : ^;^:M?s??'
tt'fyM^^WiZf-X'ySi 0. 0550 '::" :.;.?. -f^^^iJ^M^ i£:
0.0444
0.0341
0.0242
0.0148 ,..; ? ..:.,;:,::,: .;
0.0 'v;;i:.;.-:::-v;:/::.- . ' ' ;: ';V:. .H;'';1.''..
TOTAL CARBON REQUIRED = 31.12 INCHCS : ., /
TOTAL STAGES REQUIRED ASSUMING 1.65:INCHES CARBON/STAGE =18.86
SPACE VELOCITY =
4139. 1/HR
PRESSURE DROP ACROSS CARBON =
15.56 INCHES H20
PRESSURE .DROP ACROSS PLATES ~! 7.78 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = i ;23.34 INCHES H20
156
-------
S02 SORBER DESIGN
RUN NUMBER TEST-5 DATE 7 27 71
TOTAL CARBON RATE = 50.640 JJ3S/HR
0 U T L E T C AR BCN L0 AOTNG " = "0 .18 37 5~"L 8S~~ACTOTtFTARWfT
HEIGHT OF CARBON/STAGE = 4.00 INCHES
DIAMETER OF VESS_EL_ = 18_._0 INCHBS "
"CARBONi""USED"= "0. ~" " w
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION = 2000. PPM
INLET NCTCUNCENTRAT ION"=" " "T5
INLET-02 VOLUME FRACTION = 0.0460
INLET H20 VOLUME FRACTION ^ 0.1300
"OUTLET S02r CONCENTRATTON =
TEHPERATUR
|:
I STAGE
!v i
, 3
:"..: -.-:.. '' :--'--' J;r':-;':
8
. ' * 0.56
i
,-_*_ .,..-,.
E = 200.0 DEG. F
S02 CONCENTRATION ; ;
.PPM- '4w:i*-:;v:
\2000..:::"Hiif:;i
1772.
1531.
1279.
;,:.: -:::X:'.:.:. 1023.
;.;->;.;: i;,V.. -.;,.768. '
..-'"-.'::'..:::,':'. 525.
306.
200.0001
:. AC TO" LOAD ING " " ; --
LBS ACID/LB CARBON . :
:-..v:::xi. :V, :: 0. 1837 ;/' ..1: -f: '
0. 1604
0.1357
.0.1099
0.0836
0.0575
0.0326
0.0102
' 0.0
TOTAL CARBON REQUIRED ^J^J^V. 22: INCHES^ _
"tCTAL STAGES REC07"RiEO ASSUMING "4.00 INCHES~CARBON/SrAGE
SPACE VELOCITY = 3764. 1/HR
PRESSURE DROP ACROSS CARBON - 17.11 INCHES H20
P R E S S UR_1 J3R C l>_ ACR_OS S PLATES = 8.56 INCHES H20
'TOTAL PRESSURE"DROP" ACROSS STAGES = 25~.67~ INCHES H2o
157
-------
S02 SCRBER DESIGN
RUN NUMBER TEST-6 DATE 7 27 71
TCTAL CARBON RATE _= 50._6A_0 _L_BS/_H_R
"OUTLET""CARBONLOADING V~0.~1.83T5 LBS ACID/LB CARBON"
Ml: I GMT OF CARBON/STAGE = 6.00 INCHES
OIAPFTER OF VESSEL. = 18.0 INCHES ^^y^-/---^;^;:-^^. _
"CARBON" USED" = """ b.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION_= 2000. PPM
INLET" NO" CONCENTRATION"~= ~ f5bT PPM '
INLET 02 VOLUME FRACTION ~ 0.0460
INLFT H20 VOLUME FRACTION - :, 0. I3QQ
~ OUTLET'~S02~CONCWTRA"fiW = 200."
$02" CONCENTRATION: M^rf. v ACID LOADING
STAGE PPM :-:-x: M^iWilP;: LBS ACID/LB CARBON
'1 2000.:.pl||lli 0.1837
2 1663.
3 1299.
4 922.
*.-.. .:-. . ' 5 - :.v;..;'-.-:;.: :..:' ;"' .-^SSa.v^^-:;:::-::?.:::*;1::'-^:::;-::-:::;-^:-.:-.?;-.^-,.
;-: .: . - . . :-- ..-..J .-..-... :-. ....--. ---; .:......:-.... :..-: * -»v .:-.-:-:>.:-:::-:-::-:::-::::-:-:>:-.:--:/:::: :-::-r-Xv.- ,->.-,/:
; .; . ' >v.v ;;. - ; ;'... <: ;.y -:':' '.-x:' ' : . : : : -. ' '- -:.:-. - ' : .; : -:.x;.v<.:-:;:;:;:;1;1v:;:;:-'-> x-::>'-.-:- -:-1-'-:yX;>:-:-: .;:;:< : :-
I^MCo'vi^l^r:';---^v2'ob;ooo'r:^II^M^K^.
0
0
0
i 0
:;.:0
;i-::0
. 1492
.1119
.0734
.0360 :.-. .. ;,:,:.,:-.-::,, :.-,v..;::;;:,:-
.0035 ;;?;: '^^^^.'^: v? :;'
. o .::.;:-;" \i',:'r:'.x r^:K':':s-x::;':' ''....''.'??'."
36.88 INCHES
TOTAL CARBON REQUIRED =
TOTAL STAGES REQUIRED ASSUM ING-. 6.00: INCHES CARBON/STAGE =.,6.15
SPACE VELOCITY =
3492. l/HR
INCHES H20
PRESSURE DROP _ACROSS_CARBON_f__ 18.
PRESSURE" "DRCP ACROSS' PLATES =-\.:.j;-.. 9".22-."INCHES'"Hzo
TOTAL PRESSURE DROP ACROSS STAGES = 27.66 INCHES H20
158
-------
S02 SORBER DESIGN
RUN NUMBER TEST-7 DATE 7 27 71
TOTAL CARBON RATE = 50.64_p__LBS/HR
OUTLET' CA'RBON"'LOADrNG~="0.183T5 ITS'" AC TBTLB~C/AR'BON""
HEIGHT OF CARBON/STAGE = 9.00 INCHES .vT ,: ;
DIAMETER OF VESSEL = _ 18 . ?_I_N£HES , ^: : *:\: V: :
"CARBON usEi>" = ---g^ -.- -~^ -
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CCNCENTRAT10_N _= 2000. PPM
INLET NO COMCENTRAnON"= """"" ; 150. PPM"""' ~""~"
INLET 02 VOLUME FRACTION = 0.0460 ; ^
INLET H20_y_CLUME FRACTION =. :-,0. 1_300A. x/!j"^£:;.?':"':-;-;:'
OUTLET S02 CONCENTRAflbN = ""200. PP~M~ ""
J§?lp-EMiyM_= 200.0_0_EG. F
S02"CWc"ENfRAT10N AC 10 Td'AD I"N"G
STAGE . PPM LBS ACIU/LB CARBON
1 ..2000. °_«i83J_
"0."1329
0.0774
r\
I -^ \S V " "
_____
2
3
4
1504. (
962. I
438. !
TOTAL CARBON REQUIRED = 40.76 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 4.J3
SPACE VELOCITY = 3161. 1/HR
20 . 3 8'
PRESSURE DROP ACROSS PLATES = 10.19 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = 30.57 INCHES H20
159
-------
SQ2 SORBER DESIGN
RUN NUMBER TEST-8 DATE 7 27 71
TOTAL CARBON RATE = 50.640 LBS/HR _ _
"6"UtLC"fCARBON~LpA'0"lNG =' 0.113375 Lt5S AC 10/I5~CARSON
HEIGHT OF CARBON/STAGE = 12.00 INCHES
0I A Y E T E R 0 F _ V E S S E L _f_JL8_.0_ INC HES 1
"CARI!UN"USEb "= ~" 0.
TOTAL GAS FLOW RATE = 18969..SCFH
INLET SC2 CONCENTRATION = _2009'_ p_p?l_ _
INLHT NO CONCENTRATION"^ ^ "" 1"50T PPM" " "" ~~~
1NLLT 02 VOLUME FRACTION = 0.0't60
INLCT H20 VOLUME F.RACTIGN_= °JLJ^L?°_^ ,
"OUTLET S02~CG"NCENTRAnW~=~~ 200. PPM
TEMPERATURE = _200_.0 DEG_. F ' ^_
"""" S02 CONCENfRAT'lO.N ~^~ AX ID LOAD ING
STAGE V; PPM L6S ACID/LB CARBON
.:.. . ' : 1' < :':'':':: :?:D;:; ZOOO. 0.1837 . :
2 1351. 0.1173
3 650. 0.0454
0.72 200.0001 0.0
TOTAL CARBON REQUIRED = 44.67 INCHES
TOTAL STAGES REQUIRED ASSUMING12.00 INCHES CARBON/STAGE = 3.72
SPACE VELOCITY = 2884. 1/HR
PRL"SSURE_DROP_ ACROSS CARBON = 22.33 INCHES H20
'PRESSURE D'RO'P ~ACROSS"PLA"TES = 11.17 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = 33.50 INCHES H20
160
-------
S02 SORBER DESIGN
RUN NUMBER TEST-9 CATE 7 27 71
TOTAL CARBON RATE = 50.640 LBS/HR
OUTLET CARBON LOADING = 0.18375 LBS ACID/LB CARBON
HEIGHT OF CARBON/STAGE = 18.00 INCHES
DIA M E T IE R _OJ:_V E_SS_E_L_=_ 18.0 INC HE S _____
"CARBON 'USED =" " 0.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION = 2000. ?P!t__ _
INLET "NCI"~CO'NCENtR"ATlON""= I'JOi PPM:
INLET 02 VOLUME FRACTION = 0.0460
INLET H20 yCLUME_ FRACTION = 0.1300
"OUTLEt""S02" CCNCENTRATToN = 200". PPM
TEMPERATURE = 200.0 DEG. F _
"~S02"CONCENT"RATl'ON '.: '-\ ";'''' "AC I'D LdAOiNG "~"
STAGE PPM ':;::: LBS ACJD/LB CARBON
' _ I.;" .::;;. _, 2000. :::/.:i:.V'i::i:x:>:.;v ...:. .0,^837..-..:
" "2 Y666. " . 0.0880
0.93 200.0001 0.0
TOTAL CARBON REQUIRED:= :. .52.70 INCHES
TOTAL STAGES" REQUIRED ASSUMING'IS.OO INCHES CARBON/STAGE = 2.93"
SPACE VELOCITY = 2444. 1/HR
PRESSURE DROP ACROSS CARBON = 26.35 INCHES H20
PRESSURE DROP ACROSS PLATES ='/-'^ 13.17; INCHES H2D
TdfAL PRESSURE"DROP ACROSS STAGES = 39.52 INCHES H20
161
-------
S02 SGRBER DESIGN
RUN NUMBER TEST-10 DATE 7 27 71
JOTAL CARBON RATE = 50.640 LBS/HR __
UUTLbt CARSONT'OADING = 0". 13375 UBS ACID/LB CARBON
HEIGHT OF CARBON/STAGE = 24.00 .INCHES
DIAMETER OF VESSEL = 18.0 INCHES
CARBON USED = 0.
TOTAL GAS FLOW RATE = 18969. SCFH
JNLET SC2_CCNCENTRATIGN_= 20_0_0_. _PPM
INLET NO" CONCENTRATION"^"" rod. PPM
INLET 02 VOLUME FRACTION = 0.0460
INLET H20 VCLUME FRACTION = 0.1300
OUTLET S02 CONCENTRATION * 200. PPM
S02
STAGE
. ' I
2
0.48
CONCENTRATION
PPM
2000.
808.
200.0001
ACID LOADING
L8S ACID/LB CARBON
0.1837 .../
0.0616
0.0
A C ARBON REQUI RED = 59.61 INCHES
__
STAGES REQUIRED ASSUMING. oo INCHES CARBON/STAGE = 2.48
SPACE VELOCITY = _ 2161. i/HR
PRESSURE DROP ACROSS CARBON - 29.81 INCHES H20
PRESSURE DROP ACROSS PLATES = 14.90 INCHES H2Q
"TOTAL' PRESSURE DRQP'ACROS'S STA'GES~= 44.71 INCHES H20
162
-------
S02 SORBER DESIGN
RUN NUMBER
TEST-11 DATE 7 27 71
TOTAL CARBON UTE = 50 . 6VOL B S/HR
_
"OUTLHT "CARBON LOADING = 0.18375 Ll~S~~/rClWrB"Tfi"R'BflN~
HEIGHT OF CARBON/STAGE = 32.00 INCHES :;:/: v:.:::::::<.
CARBON USED = 0.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET Sp2_CCNCE.NTRATION_= _^ 2000. PPM
"INLET "NO"CCNC;ENTRAriON"-- i~5b'."r~ppM"~~
INLET 02 VOLUME FRACTION = 0.04&0 ,,''.'
INLET H20 yCLUME FRACTICN = 0.1300_
OUTLE T "502" CO'NCEN TR AT ION = 200 .TP'M
TEMPERATURE = POO.O DEC. F
.$02.CONCENTRATION
'STAGE PPM
(l 2000.
ACID LOADING x..
LBS ACID/LB CARBON
.:*'.;;., -:. 0. 1837 <"^
2
0.19
510.
200.0001
0.0311
0.0
TOFALl
TOTAL
CARBON
STAGES
_REQU_I_R_ED'
REQUIRED"
70.10 INCHES
SPACE VELOCITY =
ASSUM1NG32.00INCHES CARBON/STAGE = 2.19
1838. 1/HR
PRESSURE DROP ACROSS CARBON =
PRESSURE DROP ACROSS PLATES =
TOTAL PRESSURE DROP ACROSS STAGES -
35.05 INCHES H20
17.52 INCHES H20
'52.57 INCHES H2"0"
163
-------
502 SORBER DESIGN
RUN NUMBER TEST-27 DATE 7 30 71
TOTALL CARBON RATE = 25.320 LBS/HR
OUTLET "CAR&'CNTbAD'iN'Gi = 6.18375 LUS ACID/LB CARETON
HEIGHT OF CARBON/STAGE = 4.00 INCHES
= 18.0. INCHES
CARBON USED = 0.
TOTAL GAS FLOW RATE = 9484. SCFH
INLET_SC2_CONCENTRATION_f 2_P0.°_^ PPH.
""lNUET~N"C~CONCENTPrAfiON"- ..'-;.^-: "150". .PPM::-,"
INLET 02 VOLUME FRACTION = ^(3.0460 :r-: W;:
^LE^J^O^ VOLUME FRACT I CN - :, :.Q. 1 300J-:.: f ; !
"OUTLET su2" CCNCENTRA'TIUN = 200. PPM
TEMPERATURE = 200.0 DEC. F
S02 CONCENTRATION ACID LOADING
STAGE PPM LBS ACID/LB CARBON.
1 ' 2000. 0
2
3
4
1556.
1072.
S89.
0.1383
0.0887
0,0392
2 oo. ooo i^:;mmm$*m^ ^^ ±o. o.
TOTAL CARBON REQUIRED = 19.78 INCHES
TOTAL STAGES REQUIRED ASSUMING 4.00 INCHES CARBON/STAGE = 4.94
SPACE VELOCITY.> 3257. 1/HR
PRESSURE DRCP ACROSS CARBCN = 9.89.INCHES H20
PRESSURE DROP ACROSS PLATES = 4.94 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = 14.83 INCHES H20
164
-------
S02 SORBER DESIGN
RUN NUMBER TEST-28 DATE 7 30 71
TOTAL CARBON RATE = 25.320 LBS/HR
OUTLET CARBON LOADING = 0.18375 LBS ACIO/L8 CARBON
HEIGHT OF CARBON/STAGE = 9.00 INCHES;
DIAMETER CF VESSEL:- 18.0 INCHES
CARBON USED = 0.
TCTAL GAS FLOW RATE = 9484. SCFH
NLET S2CCNCENTRATION OO PPM
__ ___ _. _
"INLET NO "CONCENTRATION = ../; ispr PPM
INLET 02 VOLUME FRACTION = 0.0460
INLET H20 VOLUME FRACTION = ; 51 0.1 300
OUTLET S02 CONCENTRATION = 200. PPM
TEMPERATURE = 200.0 DEG. F
S02 CONCENTRATION ACID LOADING
STAGE : PPM LBS ACID/LB CARBON
;::'" ;:l::::.r-,: Ti:v'w '2000. ..0.1837 ....
2 1066. 0.0880
0.93 200.0001 0.0
TOTAL taRBONREtR'EPOX:?
TOTAL STAGES REQUIRED ASSUMING "9.00 "INCHES CARBON/STAGE = 2".93
SPACE VELOCITY - _ 2444. I/HR __ ........... __ _
PRESSURE DROP ACROSS CARBON = 13.17 INCHES H20 ^^^§^51^
-.-OROP- ACROSS .PES:-:^-:g^'::-:---6\' 5 9:. INCHES
TOTAL "PRESSURE DROP" ACROSS STAGES = 19.76 INCHES H2o
165
-------
S02 SORBER DESIGN
RUN NUMBER
TEST-29 DATE 7 30 71
TOTAL CARBON RATE = 25.320_LB$/HR
CUTLET "CARBON" LOADING"'=~~"6 Vi aaYs TBS ACID/LB CARBON"
HEIGHT OF CARBON/STAGE = 18.00 INCHES,;;,;;
DIAMETER OF VESSEL = 1.8.0 INCHES J'J*v£&*:/ii:
"CARBON'US'ED ------- o."~ "
TOTAL GAS FLOW RATE = 9484. SCFH
INLET S02_ CCNCENTRATICN_= 2.00_0_._PPM
INLET" NO" CONCENTRATION = "' "150." PPM""
INLET 02 VOLUME FRACTION = 0.0460
INLET H20 V 0 L U K' E F R A C T I CN_ = . 0. 13 00
OUTLET so2" CONCE"NTRAT"ION = 200. "PP"M~
I' "STAGE
\ .-. . 1.
0.10
:;';-:-..:/'.----. : PPM
""'. ;':;'^.-;.'' .2000,
200.0001
ACID LOADING ,
IBS ACID/LB CARBON :-
0. 1837 x -:.>/
0.0181
0.0
TOTA'L CARBON REQUIRED' -C y 37.83:-JNCHES
TO"TAL STAGES REQUiRETASsuMiNl3l8.""oo INCHES CARBON/'STA'GE = 2.10"
SPACE VELOCITY =
1701. 1/HR
PRESSURE DROP ACROSS CARBON =
PMSSURE_DROP__ACROSS_ PLATES = __
"ftiTAl"PRESSURE DROP" ACROSS STAGES
18.93 INCHES H20
9.46 INCHES H20
28.39 INCHES H20"
166
-------
S02 SORBER DESIGN
RUN NUMBER TEST-30 DATE 7 30 71
_TOTAL CARBON JATE = 25.320 LBS/HR
outLET~CAR'BON LOA'DiNG"'=" o"."i8375 "Cos ACi D/LB cA'RBON"
HEIGHT OF CARBON/STAGE = 32.00 INCHES
DIAMETER Of VESSEL _f l8_.
-------
S02 SORBER DESIGN
RUN NUMBER TEST-31 DATE 7 30 71
TOTAL CARBON RATE = 37^9_80 LBS_/HR_
"OUt LET""CARBON ' LOADTNG" =. 0/10375 LBT'ATl ~07CB~~C'AR~BO"N
HEIGHT OF CARBON/STAGE = 4.00 INCHES
DIAMETER OF VESSELV;= 1^9_JLNCJjES
CARBON USED = 0."
TCTAL GAS FLOW RATE = 14227. SCFH
INLET S02 CONCENTRATION^ _?00.P_- PPM_
INL E T "NtTCONC E N TR AT I ON = "" 150T~ PP'M".,'
INLET 02 VOLUME FRACTION = 0.0460 '
INLET H20 VOLUME FRACTION ~ Q.I 300 <
'OUTLET "S'02"CONCEN'tRATiON = 200. P'PM
TEMPERATURE = 200.0 DEC. F
?.-"" .. " S02 CONCENTRATION
I STAGE : PPM
i V 1 "'' >:":. : 2000.
2 1699.
3 1376.
4 1040.
C " >;. ,; .' :: ' 0 . 7 5 I ? . i- . , v "' ; 2 0 0 . 0 0 0 .1;':; . :«; W^
: ACID LOADING
' LBS ACID/LB CARBON
... 0.1837
0.1529
0.1198
0.0854
.i. ?: :.:::??.; -x >;;,-,..:-. -0.0512 . -..-;-::_ ...::-.::
£"#&&&:. :.:\ '.0 .0196 ::.^^i::\f ^.iv- -;;:-:
^kltSS^x?,0 * Q :?1 11^. v.:^: -₯'X\' '
TOTAL'CARBON REQUIRED = 26.99 INCHES
TOTAL STAGES REQUIRED ASSUMING 4.00 INCHES CARBON/STAGE - 6.75
SPACE VELOCITY = 3579. 1/HR
PRESSURE DROP ACROSS CARBON = 13.50 JNCHE_S H20
PRESSURE"'DRoFACRoss.PLATES = 6.75~rNCHES~"H20-
TOTAL PRESSURE DROP ACROSS STAGES = 20.24 INCHES H2U
168
-------
S02 SORBER DESIGN
RUN NUMBER TEST-32 DATE 7 30 71
TCTAL CARBON _RATE__^_37_. 980 LBS/HR
OUTLET "CARBON "LOADING = 0. l8375"~LBS~
HEIGHT OF CARBON/STAGE = .9.00 INCHES:
DIAMETER OF V ESSEL_= 18.0 INCHES
"CARBON USED"=~~" " bT"
TOTAL GAS FLOW RATE = 14227. SCFH
INLET S02 CONCENTRATION^ 2A00- f?M
"INLET W"CONCENTRATrdN>. " ....150.""PPM
INLET 02 VOLUME FRACTION = 0.0^60
INLET H20 VOLUME FRACTION - .0.1300
" SO 2" CONCENTRATro.N" = 20"6~.
OUTLET
TEMPERATURE = 200.0 DEC. F
" " " ~~ S02l'C 0 NC E N TR A T" I ON"
STAGE s; PPM
;'- <:: i4l?i.tFi;f>: 2000.
2
3
0.72
" ~~"A"CTO~ro A D FN1S"
LBS ACID/LB CARBON
650.
200t0001
OV1173
0.0454
0.0
TCTAL CARBON REQUIRED = 33.50 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 3.72
C SPACE VELOCITY =
2884. 1/HK
PRESSURJLP_ROP ACROSS CARDQN -
"PRESSURE DROP""ACROSS PLATES =
TOTAL PRESSURE DROP ACROSS STAGES =
6^75__I NCHES__H20
8.38 INCHES H20
25.13 INCHES H20
169
-------
S02 SORBER DESIGN
RUN NUMBER TEST-33 DATE 7 30 71
TOTAL CARBON RATE = 37.98p__L_BS_/HR __
OUTLET" CARBON LO~A~DTNG'"=~0. 183~75 "LliS TCTD/LB C'A~R"B~0~N
HEIGHT OF CARBON/STAGE = 18.00 INCHES
C 1 AMCTER_ 0F_VESSEL « 18_. 0 1NCHES_^______
'CARBON USED "= 0."" ~
TOTAL GAS FLOW RATE = 14227. .SCFH
INLI:T SC2 CONCENTRAT I ON_= 2000. PPM
"INLET NO ""CCNCENTR'ATION"*~ fso'T'ppM
INLET 02 VOLUME FRACTION = 0.0460
INLET H20_ VOLUME FRACTION = 0. 1300
'OUTLET "S02 CCNCENTRATION = 200. PPM
ERATURE = <
S02
STAGE
1
2
0.48
?00.0 DEC. F
CONCENTRATION
PPM
2000.
808.
200.0001
ACID
LBS ACI
LOADING
D/LB CARBON
0.1837
0.0616
0.0
TOTAL CARBON REQUIRED = :: : 44.71 INCHES; ____ __ __ ___
STT AGES' REQUrRED TSSUMINGIS.OO INCHES CARBON/STAGK =
SPACE VELOCITY = 2161. l/HR
PRESSURE DROP ACROSS CARBON =: 22.36 INCHES H20
PR_ESSyRE_DRCP ACR_OSS_ PL AT_ES__=__ _^_1_1_._18 _INCHES H20
"TOTAL" P"RESSUR"E"D"ROP'ACROSS STAG'ES = "" 33753 TNCHE'S H2"o
170
-------
S02 SORBER DESIGN
RUN NUMBER TEST-34 DATE 7 30 71
TOTAL CARBON RATE = 37.980 j-BS/HR
"OUTLET"" CARBON TOADlNG = O.Tel 75 "LlS ACID/LB"~CAR"BON
HEIGHT CP CARBON/STAGE = , 32 , 00 INCHES \ .:.
DIAMETER OF VESSEL = Ij.O INCHES ^/^.X&^Z"::-.'. :.': ': ."' ''..
' '~'~
TOTAL GAS FLOW RATE = 14227. SCFH
INLET_S02 CONCENTRATION =_ __ 200p._P_P_M
INLET NO "CCNCFNTR'AtiO'N "-" " "Tl50T PPM"
INLET 02 VOLUME FRACTION = 0.0^60 . ::
INLET H20 VOLUME FkACTiqN_^ __ 0_. JL 3D 0_ £^_
OUTLET $02 "CONCENTRAI 'ION" = "200. "PPM
STAGE
1
2
0.00
S02 CONCENTRATION .':
PPM
2000.
204.
200.0001
ACID LOADING
LBS ACID/LB CARBON
0.1837
0.0
. 0.0
TOTAL STAGES REQUIRED ASSUMING32.00 INCHES CARBON/STAGt = 2.00"
SPACE VELOCITY = 1508. 1/HR
PRESSURE DROP ACROSS CARBON = ; r:: :i'32.03'::INCHES H20
PRESSURE DROP_ACRpSS_ PLATJES = Y 16 « 02^ I NOME S H20
TcfTAl PRESSURE"~DROP ACRCSS "SFAGES" = 48.o"5 INCHES H20
171
-------
APPENDIX A-9-2
EFFECT OF THE LINEAR GAS VELOCITY ON THE TOTAL CARBON
BED DEPTH REQUIRED TO REMOVE 90% OF AN INLET S02
CONCENTRATION OF 2000 PPM
Carbon Bed Depth/Stage,
inches Run Number
4 Test-27
4 Test-31
4 Test-5
9 Test-28
9 Test-32
9 Test-7
18 Test-29
18 Test-33
18 Test-9
32 Test-30
32 Test-34
32 Test-11
172
-------
S02 SOR&ER DESIGN
RUN NUMBER TEST-5 DATE 7 27 71
TOTAL JDARBON RATE = 5C
""OUTLET CARB'CN TOADfNG = 6.1B37~5 LBS A CID / L B CTfTBOlTTr
HEIGHT OF CARBON/STAGE =
JD IA M E TER _OF VESSEL = 18''.(
CARBON USED = 0.
TOTAL GAS FLOW RATE = 18969. SCFH
J_NL.^T._1°1__C°.NCFIIRAJJ ON = 2000._ PPM ___________
I"NLET NO CCM^ENTR'At IO"N" = ..:,:: .,-, 150." V9]^^:::<^:-.:^amK
.. INLET 02 VOLUME FRACT ION := vifl ' '":'"':>*--^>"> »----
INLET H20 VOLUME FRACTION :=;::-.
"OUTLET~S02"CONCE"NTRA"Tro.N =
TEMPERATURE = 200.0 DEC. F
20 0. TPfi
|" S02
I STAGE
I , I
2
3
4
CONCENTRAT
PPM :/;;;;:£
1772.
1531.
1279.
ION -::v-x.:;v:::-::-.#- V AC 1 D . LOAD I NG >.i- v:^-:::.:*^-::;.- ''*".
:;:|:::J|||g::;;.LBS AC 1 0/LB C ARBON: V/^^lf |i|«>'<:S>
0.1604
0.1357
0.1099
56
306.
'200.0001
0.0102
0.0
TOTAL CARBON REQUIRED >=?; ::.:; :: 34;22 JINCHES;
TCTAL STAGES REQUIRED ASSUMING 4.00 INCHES CARbON/STAGE =8.56
SPACE VELOCITY =
3764. 1/HR
PRESSURE DROP ACROSS CARBON; =
PRESSURE DROP ACROSS PLATES =
TOTAL PRESSURE DROP ACROSS STAGES =
17.11 INCHES H20 :5:»-»::«:i*-;₯V:V
8.56;!::;INCHES H20^.:W:^
25.67 INCHES H20
173
-------
S02 SORBER DESIGN
RUN NUMBER TEST-7 DATE 7 27 71
TOTAL CARBO_N JUTE = 50.640 LBS/HR
IJUTTETCARBON LOADING = 0.1837.5 LBS /
HEIGHT OF CARBON/STAGE = ;,9.00 INCHES
;TER OF VESSEL = is.o
_.
CARBON USED =~ 0.
TOTAL GAS FLOW RATE = 18969. SCFH
NLETS02 CNCENTRATION = 2000. PPM
INLET" NO" CONCENTRATION -. -:.;. ,,, 150.,PPM .
INLET 02 VOLUME FRACT ION.,=:?; '0.0460;wMiHl
. 1NLET_JJ20^VCLUME FRACTICiN ~ >.Q.
"OUTLET s"o2 CONCENTRATION = 200. PPM
TEMPERATURE = 200.0 DEC. F
2
3
4
1504.
962.
438.-
0.1329 1
0.0774 /
0.0237
200,OOCl - 0.0
TOTAL CARBON REQUIRED = 40.76 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 4.53
PRESSURE DROP ACROSS CARBON = 20.38 INCHES H20
PRESSURE DROP ACROSS PLATES - 10.19 INCHES H20
TOTAL PRESSURE DROP ACRCSS STAGES = 30.57 INCHES H20
174
-------
S02 SORBER DESIGN
RUN NUMBER TEST-9 DATE 7.27 71
.'- -. ' " -V
TOTAL £ARBON RATE - 50.640 LBS/HR '_
WTLET CARBaTTLOAblNG = 0.18375 ~LBS ACID/LB... CA~RBON
HEIGHT OF CARBON/STAGE:= 18.00
DIAMETER OF VESSEL =18.0 INCHES
CARBON USED = 0.
TOTAL GAS FLOW RATE = 18969. SCFH
JNJ-.ET__Sp2. P.CNCENTRATl ON = 2000. _____
INLET NO CONCENTRATION = .;;.:;;,,. ISO. PPM .
INLET 02 VOLUME FRACTION - ;0.0460
INLET H2p_VC_LUMC FRACTION = " 0.1300
'OUfLEf~S"02 CCNCENTRAT I ON = 200. PPM
TEMPEP.ATURE_= _200_^0 DEC. _F
S0~2 C 0 NC E NTR AT I ON aiiiif ^ > AC 10 LCTAOING"
STAGE PPM l|p:?:i,;BS;.ACID/LB .CARBON
1 2000. ^i^i^ili^iiiK?"'-b_»_l_837.'^''^
f~~2 "~^*^~" 1066. 0.0880
0.93 200.0001 ^0»0
'TOTAL STAGES REQUIRED ASSUMINGIS.OO INCHES CARBON/STAGF. = 2.93
x '' *
SPACE VELOCITY = 2444. 1/HR .
w. ,,
^PRESSURE DROP ACROSS CARBON = 26.35 INCHES H20
^PRESSURE DROP ACROSS PLATES =:::::?i 13.17 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = 39.52 INCH'ES H20
175
-------
S02 SORBER DESIGN
RUN NUMBER TEST-ll DATE 7 27 71
TOTAL CARBON RATE = 50.640 LBS/HR
"CARBO'N USED = o.
TOTAL GAS FLOW RATE = 18969. SCFH
_!NLET_SG2_CCNCENTRATION = 2000. PPM
~I"NLET~NO"CCNCEN"TR"ATION - ;.
INLET 02 VOLUME FRACTION =
INLET H20 VCLUME FRACTION^ V
"OUYLTT S02 CONCENTRATION = 200. PPM
TEMPERATURE = 200.0 PEG. F
TOTAL STAGES REQUIRE'!) ASSUMING32.00 INCHES CARBON/STAGE = 2.19"
SPACE VELOCITY = 1838.;l/HR
TOTAL PRESSURE DROP ACROSS STAGES - 52.51 INCHES H20
176
-------
S02 SORBER DESIGN
RUN NUMBER TEST-27 DATE 7 30 71 ':'--.;?'oV'
T(?TAL CARBON RAIL- =25*320 LBS/HR '
"OUTLET" CARBCN LOADING = 0.18375 UBS ACID7TO CARBW
HEIGHT OF CARBON/STAGE-; <: 4 00 INC H E S, i. ^^. iAfe-':V!
D IAMET V.R OF VESSEL = 18.0 ' INCHES -i-' ^.:.}&%::&±>^&*-£
CARBON' USED = o.
TOTAL GAS FLOW RATE = 9484. SCFH
INLET _S02 CONCENTRATION _= _ 2000. PPM __
TNLET^NC CONCENTRATION^ :::;F 'T5"0. PPM""
INLET 02 VOLUME FRACTION =! 0.0460
JNLET H20__VaLyME FRACTION -0.1300
OUT LET'S 02 C"CNCEN"fRATrD"N = 200". PPM
TEMPERATURE = 200.0 OEG. F
: ,:::::S02::CONCENTRATION;:?:.::J;:;:;l:::V ACID LOADING ,:
r:::^-:;;::^ LBS ACID/LB CARBON:
^^M^fi''l&^;^lp^o'ob^:Pf::^P ,- .: ., o.ios?.-:^
" " 2 ' ll56^ "'^^ T^TT 571383
3 1072. -'' 0.0887
4 589. ' 0
TOTAL CARBON REQUIRED = 19.78 I~NCHES
TOTAL STAGES REQUIREDASSUMING 4.00 INCHES CARBON/STAGE = 4.94
SPACE VELOCITY * 3257. 1/HR
PRESSURE DRCP ACROSS CARBON = 9.89 .INCHES H20
PRESSURE DROP ACROSS PLATES - 4.94 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = 14.83 INCHES H20
177
-------
S02 SORBER DESIGN "
RUN NUMBER TEST-28 DATE 7.30 71
IP!- CARBON RATE = 25.320 LBS/HR
1 U I M ^ ^* *S I '» L* V> I » I * >~1 l~ «_^w_*fc.** l».brvf---i ^ ^
TuTLET"C~ARBON LOADTNG = 0.18375 LBS AC 1D / L8 C AR BOlT.: .V ;:::,:.:,,;;:
HEIGHT OF CARBON/STAGE = 9.00 JNCHE.S/:;;:^;;::^
DIAMETER. CF VESSEL'' =.,18.0 INC^ESfe-fe^^ **:?-vl
CARBON US'EO = 0.
TOTAL GAS FLOW RATE = 9484. SCFH
J NkEI__S°2 CC.NCEN'TRAT K1J1 2000. PPM
"INLET NO CONCENTRATION = ;.,;::^':;r,i5p.:..ppK~,
INLET 02 VOLUME' FRACTION =^-^'^Q^bQ:;:^^^;^^i^^'-^-:^^. ||;f4
yCLUME FR ACT I GN "-'::V-;'Q. Vsob;--^'-:^^ f3g
"CONCENfRATION = 200. PPM
TEMPERATURE =200.0 DEC. F
S02
STAGE
i
2
0.93
CONCENTRATION
PPM
?000.
' 1066»
200.0001
ACID LOADING - .;: .; ..-. :.<,.;&
LBS ACID/LB CARBON : : -v ;^i;::;
0.1837 :::"-s ''«':*:-:-;
0.0880
' 0.0 _;.
..;,::::::.;:>;.:
\'.-:: -:.>-';! ::
....: .;:.::;:>:. '
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES- CARBON/STAGE = 2.93
SPACE VELOCITY = 2444. 1/HR
'PRESSURE -DROP ACROSS
^W
::H.NCHEs-/H2o;:':--;;;;.:i:--:i-::t1|D^:l^
£':. PRESSURE 0R0P ACR0SS PL ATE'S> -"---
19.76 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES =
178
-------
S02 SORBER DESIGN - -
' ''"*-.
RUN NUMBER TEST-29 DATE 7 30 71
RATE = 25.320 LBS/HR
OUTLET CARBON LOADING = 0.183~75 LBS ACtD/LB CARBON
HEIGHT CF CARBON/STAGE; = 18.00 INCHES;;^;;.^:!^^^'-:
J)IAPETER_ CF VESSEL = . 18.0 . INCHESj^MflllB"'"
CARBON LIlTED = " 0.
TOTAL GAS FLOW RATE = 9484. SCFH
INLET S02 CCNCENTRATIQN = 2000. PPM
150. PPM
INLET NO CONCENTRATION = :
INLET 02 VClUME FRACTION =^
INLET_ H20 VOLUME FRACTICN = ^,0>1300
"bUTlET S02 CONCENTRATION =
200. PPM
TEMPERATURE = 200.0 DEC. F
J STAGE
i i
2
0.10
S02 .CONCENTRATION
PPM
e . 2000,
383.
200.0001
.ACID LOADING : . SH: -;v./^:, .
iLBS AC I D/LB CAR&QU^rV-^^" ::'v
, ,, - 0'k1837'^t^^is^V^-'.)V.
0.0181
0.0
TOTAV'STA&ES REQUfRED ASSUM1NG18.00 INCHES CARBON/STAGE = 2". LO
SPACE VELOCITY = 1701. I'/hfR' = - -
PRESSURE DROP ACROSS-CARBCN =
PRESSURE DROP ACROSS PLATES":,-
18.93
9.46 INCHES.
TOTAL PRESSURE DROP ACROSS STAGES =
28.39 INCHES H20
179
-------
S02 SORBER DESIGN '. ., ... ' .
RUN NUMBER TEST-30 DATE 7 30 71 ''. -V"':-
TOTAL CARBON RATE = 25.320 LBS/HR '
~OUtiL'ET"CARBCN LOADING = 0.18375 LBS ACIO/LB CARBON
' "'
HEIGHT OF CARBON/STAGE '- 32.00 i,,v,,,^- ,, ::,,::;: ,,:.:;,::.. :,-.:
_DI AKEY £R_0 F__VESSEL ='"'18.0 .INCHES *::^^Mi%^^l^,-{i$?'Z
CARBON USED = 0.
TOTAL GAS FLOW RATE = 9484. SCFH
INLET_SC2 CCNCENTRAT10N =2000. PPM
"TNLET NO "CONCENTR'ATHTN" = :;:::; -.156.: PPM..;;;
INLET 02 VOLUME FRACTION =-0.0460 i',:^'^
_l N.LE.I H20_yCL UME FR AC T IC N_ =' ''<) ^ 1300 -y::;:;:-:!:
bUT"LE"r'Sb2 CONCENTRATION = 200."~PPM.
TEMPERATURE = 200.
.:. ,,:.::,S02 CONCENTRATION ACID LOADING
: . ., ?iPPM LBS ACID/LB CARBON
:: : :^:.-V2000. 0.1837
0.67 200.0001 . 0.0
t'-'TOTAL CARBON 'RE"CUIRE'D.-.:;=S; #&5^
I0TOTAL STAGES REQU IRED ASSUMING32..0,0 ...I.NCHES':: CARBON/STAGE =1.67:
* ' " --'." * ' i > .
SPACE VELOCITY = 1206. 1/HR -.',
?.:' PRESSURE DROP ACROSS CARBON.^^''r. 26.71 INCHES H20 ;,;,;;; :;;y;.,i:;.;
|:i PRESSURE DROP ACROSS 'PLATESf^ij1^ 13.36:;; INCHES H20 '»''"$^i*?*;KJ
PRESSURE DROP; ACROSS -STAGESl^^WiQl^.INCHES. H20- g^ : x
180
-------
S02 SORBER DESIGN ,
RUN NUMBER TEST-31 DATE 7 30 71
TOTAL_£ARB_ONI _RA_TE _~ 37. 9130 I.BS/HR
"OUTLET CARBON LOTOffiG = 0»l₯375 L₯
HEIGHT OF CARBON/STAGE >: :4.00INCHES:
DIAMETER OF VESjELs:- 1816.' INCHES?-;fi;:y;U^
CARBON USED = 0.
TCTAL GAS FLOW RATE = 14227. SCFH
INLET Sp2_CONCENTRATiqNI_=_ 20°°' _pf.M
"iNLET'NO CONCENTRATION = ... .^1507 PPM"
INLET 02 VOLUME FRACTION <:x0.0460:i::H :.:"
INLET H20 VOLUME FRACTICN -"" 0.1300
OUTLET "S02 CONCENT RATION"_ = 200. "PPM
TEMPERATURE_=_200.0 DE_G_.__F
S02"CONCENTRATION ' ~"AC ID LOADING"
.STAGE PPM LBS ACID/LB CARBON
1^ 2000.. 0.1837 :M'^
" 2 1699". ' 07T529
3 1376. . 0.1198
4 1040. 0.0854
J^n^r^lll^:l»:C:',7p6',;:;;;:;; ^:isMii&M::'6.ObiYW^.
!?::;li?Mv.>.397'£::::::
OTAL CARBON REQUIRED .'<::- .v^ 26.99: INCH'ES .v
TOTAL STAGES REQUIRED ASSUMING 4.00 INCHES
SPACE VELOCITY = 3579. l/HR
_P_RESSURE DROP ACROSS CARBON = 13.50 INCHES H20
" PRE:SSURE""OROP ACROSS PLATES = -^^ b.js INCHES. H2ti: -/;,;,w^«.;
"- TOTAL PRESSURE DROP ACROSS: STAGESV=^.v^:!::70^24.>.INCHES;-H2g:WI:ij
181
-------
$02 SORBER DESIGN
RUN NUMBER TEST-32 DATE 7 30 71
TCTAL CARBON R.AJJ_=_AI^.M5 J^M/Jl?. __
"OUTCEfCARBON LOADING -~:" 0 .1 8 3 7 5 L6S ACTp/LB
' OUTl ET'CARBON LOADING ~":" 0 »18 3 7 5 L6S .ACTp/LB"CAR00"N ... ..,-...; s::UV .'.:.;,;
HEIGHT OF CARBON/STAGE = -.9.'00 .l^ES^^;^^^^-^?.^}-^^^^
^_DIAKETER_ 0F V ESSE L - -,' 18 . 0 'I NC'HE S ;::::.;;:gg;|||g||||i|g
rADUfiK»iicPn= n.
CAR13UN USED = 0.
TCTAL GAS FLOW RATE = K227. SCFH
JNLET S02 CONCENTRATION = 2000. PPM
"rNLE"t"NO'~C6NCENTRATlON = ,:> i'.JLSO. ;PPM .j.
INLET 02 VOLUME FRACTION .'v
INLET H2p__yj]LUME FRACTION -T
"onuYLErsoT"l;"o'NcTNrRATroN~= 200. PPM
TEMPERATURE = 200.0 DCG» F
..... S 0 2 .. C 0 NC E N TR A T I'D N.J-;- .:. ! >f C iixl % : A CTD LOADTNG
--^^^^^^
CARBON ':;-:"''':^::'^iii|li!^
V^Si^
2 351. 0.1173
3 650. 0.0^54
0.72 200.0001 ' 0.0
TCTAL CARBON REQUIRED = 33.50 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/(ST«GE = 3.72
~ ?e 84 . i /HR ' !^^^^mf&n^£^^^-2-^f^^^^m
PRESSURE DROP_ACRGSS _
'PRESSURE DROP ACROSS' PLATES = 8.38 fNCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = . 25«13 INCHES H20
182
-------
S02 SORBER DESIGN
RUN NUMBER TEST-33 DATE 7 30 71
TOTAL CARBON__RAYE ^37.980 LBS/HR
"OUTLET "CARBON LO AIDING = 0.18375 TBS
HEIGHT OF CARBON/STAGE.= 18.00 INCHES:
C IAMETER OF VESSEL... - . 18.0 INCHES-;:::-::::.-.-.-.>H^M^^^I^
. . _ _
"CARBON USED = 0.
TOTAL GAS FLOW RATE = 14227. SCFH
I NL E T_ S C <1_CONC E N T R A T I ON = ___ 2 OOP. P P M
"rNL'Et NC" CONCENT RA'TTON =::,.;. ' 150.. PPM
INLET 02 VOLUME FRAC.T ION =: 0.0^60
INLET H20 VOLUME TRACTION --
OUTLET S02 ~f.C~NCENTRATl6'N =
TEMPERATURE_=^_2p_0.0 DEGJL_F
SU2,CONCENTRATION.
STAGE
r
0. 1300
200. PPM
::x ::: AC I D L0ADI NC'."-':: -j
LaS ACID/LB CARBON
0.1837 :::
2
0.48
808.
200.0001
0.0616
0.0
"TOfAL STAGES REQAHRED ASSUMING18.00 INCHES CARBON/STAGE = 2.4T
SPACE.VELOCITY = 2161 c i/HR
PRESSURE
PRESSURE _. ^ ^_ , _.
TOTAL PRESSUfiiE DROP ACROSS STAGES - 33.53 INCHES H20
183
-------
S02 SORDER DESIGN
RUN NUMBER TESY-34 GATE 7 30 71
TOTAL CARBON JA_TE = 37.980 LDS/HR
~CUTL£f"CAR80N LOADING = 0.18375 LUS AC1D/LB CARBOTT
HEIGHT Or CARBON/STAGE = 32.00 INCHES..>;....^::«:-::4':;,:u:ij|>
DIAMETER CF VESSEL = 18.0 INCHES :.. ry^iXBijiffiV:U^li^.
'CARBON USED = o.
TOTAL GAS FLOW RATE = 14227. SCFH
INLET SO? CONCENTRATION = 2000. PPM
TNLET" NO" CONCENTRATION' = ;: .. :150". PPM,.:.:.;::
INLET 02 VOLUME FRACTION = r 0,0 4 6 0 :^'^&f;
INLET H20 VOLUME FRACTION =; V0.1300
OUTLET S02 CONCENTRATION^ 200. PPM
TEMPERATURE - 200.0 DEC. F
STAGE
2
o.co
S02 CONCENTRAT ION ;;::i:;: : y:
pp^'-^KM^M^s
204.
200 ..rtnni
/::.ACID LOADING ,,; ;.' ':.,. :;£;$&& v: -A:
ISVAC'ID/LB CARBON ."V: ₯^-j^S\^,
ilSIIO '0.1837: -v, ' ; ':^*9#£%$$.?%
0.0
. 0.0
TOTAL CARBON RECUIRED;'-.%; ,:.:V64.07 :INCHES'".^^^
TOTAL STAGES REQUIRED ASSUMING32.00 INCHES CARBON/STAGt = 2.00
SPACE VELOCITY = X508. 1/HR
PRESSURE DROP ACROSS CARBON = 32.03 INCHES H?.Q
PRESSURE DROP ACROSS PLATES -: :" i ISiO^VkNCHES H2(f
TOTAL PRESSURE DROP ACROSS STAGES - ^8«OS INCHES H20
184
-------
APPENDIX A-9-3
EFFECT OF THE INLET 02 CONCENTRATION ON THE TOTAL CARBON
BED DEPTH.REQUIRED TO REMOVE 90% OF AN INLET S02
CONCENTRATION OF 2000 PPM
185
-------
S02 SORBER DESIGN
RUN NUMBER TEST-7 DATE 7 27 71 .
TOTAL CARBON RATE = 50.640 LBS/HR _ _ "
~bUTrET"CAR"BWTOADING = 0.1837.5 IBS AC IJD/LQ CARBON" ..".,;.,i...:;.;..., .v.......,:;.. ,
HEIGHT OF CARBON/STAGE > -.;C:..9.00' INCHES '^MKiif^&^^fQ^M^^y
_PlA-NEJLIB. _OF VESSEL = 18.0; INCHES . .; . . ffxrlfe;;^
TA'RBON USED = "o.
TOTAL GAS FLOW RATE = 18969., SCFH
INLET S02 CONCENTRATION = 2000. PPM
INLET 02 VOLUME FRACTION = . . ^0 . 0 A 6 0
. __
OUTLET S02" CONCENTRATION
TEMPERATURE = 200.0 PEG. F
2 " 1504. 0.1329
3 962. 0*0774.
4 -'tjC. O.G237
TOTAL CARBON REQUIRED = 40.76 .INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 4.53
^: :S P AC E' VELCC IT YH='f:: ;-^
PRESSURE DROP ACROSS CARBON - 20.38 INCHES H20
PRESSURE DROP ACROSS PLATES = 10.19 INCHES H20
TOTAL PRESSURE DROP ACRCSS STAGES = 30.57 INCHES H20
186
-------
S02 SORBER DESIGN
RUN NUMBER TEST-12 DATE 7 27 71
TOTAL CARBON RATE = 50.640 LBS/IIR
'CUTLET CARBON LOAOfNG"'=" O'.'l 037fi" L TiS ~AC IDYCTfCARBON"
HEIGHT OF CARBON/STAGE = 0.00 INCHES
DIAMETER OF VESSEL ~ 1_8»0 INCHES _ i __i __
CAR BUM USED - 67 "~"' "~
TOTAL GAS FLOW RATE = HJ969. SCFH
INLET S02 CONCENTRATION = _ 2000. PPM _
INLET NO CONCENTRATION^ "~" ~150'.~P'N"",~. 3""~
INLET 02 VOLUME FRACTION = 0.0200 :; .;>:: ::
INLET H20 VOLUME FRACTICN ^..^l-iOp, ; ________
"OUTLET s'o'2 CONCENTRATi'dN""= " " 20b.~"pp~M
TEMPERATURE = 200.0 DEC. F
S02. CONCENTRATION , ACID LOADING ~'
STAGE PPM : ::::,:; ;:;'';: LBS ACID/LB CARBON
" ':^^--^^--:'.. ^.. o.
&' _iii'- ;^^ i.1^^. Uu_. -_
2 1699. 0.1530
3 1377. 0.1199
4 1041. 0.0855
TOTAL CARBON REQUIRED = ' 60.80 INCHES
TOTAL ST'AGES REQUIRED ASSUMING 9.00 .INCHES CARBON/STAGE = 6.76
VELGC I Y 2l9.
PRESSURE DROP A C R 0 S S C A R B ON = 30. 4 0 INC H E S H2 0 __ m_
"PRESSURE" DROP" "ACROSS "PTAT"ES""=" 15.20 INCHES H20
TOTAL PRESSURE DRCP ACROSS STAGC-S = 45.60 INCHES H20
187
-------
S02 SORBER DESIGN
RUN NUMBER
TEST-13 DATE 7 27 71
TOTAL CARBON RAJEjf_ 50.640 JJISVHR
~ffUfL'Ef""CA"RB6N""LOAOINe""=""oTl8375 IBS ACTDTLB CARBW
HEIGHT OF CARBON/STAGE = 9.00 INCHES
_D I A ME T ER_ C F_V E S S E L JL 19 . P_J.NCHE_S__ ,
CARBON USED = 0." """
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CCNCENTRATICN_ = 2000. PPM
""INLET" NO"CONCENTRATION""= 1~50T"~ "
INLET 02 VOLUME FRACTION = 0.0300
INLET H20_VCLUME FRACTION =0.1300
"OUTLET S02~ CONC'ENTR'AT'TON"* "200T
PPM
PPM
STAGE:
!>;'
2
3
4
.,- "-,5v.-;-
^/v0.53;:-.-,v:
S02 CONCENTRATION
PPM
-.:! .2000.
1616.
1199.
773.
:. -:.V:,-:-. »- - 378. .:-:-::/:
;-:- 2 oo. ooo i M-S
ACID LOADING ^
LBS ACID/LB CARBON :;
0.1837 '".. '; . ..;,,..:
0.144A
0.1017
0.0580
mm^, ::::c;,, .. o.or/6.,.^._,-::.-.. ........
WZSvtst. i.:;: :?*;:*%*£ Jv 0.0 '' ^-'- ' ' 'A^:- K-S'* '> '»' '' '"
myV!-ffiKX^M;Vf
-------
S02 SORBER DESIGN
RUN NUMBER TEST-14 DATE 7 27 71
!PJ"AL C.AR!i.ON_RA-lE "... 50*640 LBS/HR
"OUT"L"ET~C"A"R₯ON""LOAOING =; o. r83"75~TB~s~ AC 1 D/FBTARBON"""
HEIGHT OF CARBON/STAGE = 9.00 INCHES
_D IAMETER_ eF_Vj[SSE L = 18.0 INCHES '
CARBON~usED = o.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION^ __2000. PPM
"INLET"NCTCONCENTRATTON" = " " i"5C)7
INLET 02 VOLUME FRACTION = 0.0600
INLET H20 VCLUME FR_AC_TICN = 0.1300
OUTLET "S02" CCNC'ENTRA'T i'0'N "= " 200 .
TEI*
f:-;--. -.'.'
|- :,.- ;.
1PERATUR
STAGE
:,; . l>
2
3
4
0.05
,E = 200.0 DEC. F
S02 .CONCENTRATION
PPM
2000.
1419.
788.
223.
:..::: 200.0001 :Vx:;:::::v-::
ACID LOADING : ;
LBS ACID/LB CARBON ' ;V
o. 1837 . . .;; .;.''"..; ;.:-{'.-K:
0.1243
0.0595
0.0017
:.:.::::.'., ..-^- ::;...: ;.. 0.0 .. .' . . .:f:; ;;:
TOTAL CARBON REQUIRED = 36.42 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CAR B3N/ STAGE = 4. 05
SPACE VELOCITY,*
3537. 1/HR
PRESSURE DROP ACROSS CARBON * 18.21 INCHES H20
PRESSURE DROP ACROSS PLATES 9.11 INCHES H20
TOTAL PRESSURE DRO.P ACROSS STAGES » 27.32 INCHES H20
189
-------
S02 SORBER DESIGN
RUN NUMBER TEST-15 DATE 7 27 71
TOTAL CARBON RATE = 50^640 LBS/HR_
'CUTLET ' CAR'NCN LOA'D1'NG~ = " 6 . 1 8 3 7 5""L JJS~7kin'TJ7 L B . CWfl'ON""
HEIGHT OF CARBON/STAGE = 9.00 INCHES
DIAMETER U F V E S S E L = 18 OWCHES
CARBON
TOTAL
INLET
INLET
INLET
INLET
OUTLET
USED = 0.
GAS FLOW RATE =
S02 CONCENTRATION =
NO CONCENTRATION =
02 VOLUME FRACTION
H20 VOLUME FRACTION
S02 CONCENTRATION
18969
= 0.
=
. SCFH
2000. PPM
1000 :,;;: 'v:';:;-':i; :';>:; ...
200. PPM
TEMPERATURE = 200.0 DEG. F
i; STAGE
! " ' :; 1
2
3
0.2»
S02 COivCr-NTRATlOM
PPM
2000.
1220.
403.
200.0001
ACID LOADING
LBS ACIO/LB CARBON
0.1837
0. 1039
0.0201
0.0
TOTAL CARBON REQUIRED = 29.51 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 3.28
SPACE VELOCITY = ^365. 1/HR
J?.RE_SSyRE_DROP ACROSS CARBON - :: 14.76 I NCHES_^H20_
PRESYUR~£ DROP'TCROSS PLATES = " 7.38"""l"NCHE"S H20
TOTAL PRESSURE DROP ACROSS STAGES = 22.13 INCHES H20
190
-------
APPENDIX A-9-4
EFFECT OF THE INLET H20 CONCENTRATION ON THE TOTAL
CARBON BED DEPTH REQUIRED TO REMOVE 90% OF AN INLET
S02 CONCENTRATION OF 2000 PPM
191
-------
S02 SORBER DESIGN .
RUN NUMBER TEST-7 DATE 7 27 71
TOTAL CARBON RATE = 50.640 LBS/HR
T)UTrErcTRBON"TnAING =. 0.1837.5.-.LBS AC I D/.LB CARBON
HE IGHT 'OF CARBON/ STAGE * '
DIAMETER OF VESSEL '= 18 .0
CARBON USED = 0.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION = 2000. PPM
INLET NO CONCENTRATION -.
'150.
INLET 02 VOLUME FRACT ION . =l:;.OV0460-i!^^|;|||i§|||g^^
INLET H20 VCLUME FRACTION =:,::>: 0i" 130&iK^jSM^MMJm
"OUTLET 502 CONCENTRATION =
TEMPERATURE = 200.0 DEC. F
200. PPM
.502 CONCENTRATION.
ACID LOADING
0.53:Ma:.::.::.U:200.0GOI
;:;;;.;:-::| ;.0.0.j:g
STAGE
1
2
3
4
PPM
2000.
1504.
962.
LBS ACID/LB CARBON ^^Xtf*^ '" -:
:;-v:V:'.: - 0.1837 ''' :: '''''"'?'' :*-"'A:S-:V. :."'
. ,. -:'-v';V ."»«-' -::.-.;, ..-.:.:. v':- ::' -'..-"
0.1329
0.0774
0.0237
TOTAL CARBON REQUIRED = 40.76 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 4.53
;.;.; ...;.'.; ::.-; ';; y^-'.ViY
SPACE VELCC
;:.:-. . /. ;- : .-;>-.;..;.. ,:
. . . -: --..
.'.-. '';-.';'.'. '.'..'.'.,..::-'.'.;' .'.-..','..' .".'
:TY:..= --':'--:;:'iK3l6'ii'
' v-.V/'ir i:.--'-: V' J:?:::W::.:^:::!':';"::''' -.:".
.-- . - .--- -:..:-.
:;:J:s:.':;s:?;
1/HR:
:-::';:-:::;:':
;|;|?;::;s.;;:|::.v.
;;;x:;;;;-.;::.j:i:?S;j;2x
.':'.'':'£"'' '.'.'?'''x'x':'.
:';::-::: ':. .;::>::
f&:-V£tifK
ii:₯Siffii-i£:!-i?::;%
Jiiggi:;; :':"»:
'. ! .-", '':'- ' '' '.
£^&&£?g$*.^t
;-;:.;i;:.:.::::;: ^;^3x££'& ^^l
;>:;:>:>. ';V'1::'".:;v;:''';::'"':'OX''::::;:;':-t':*
'' ; -'- '':';-'/-.:.:v ;':.' ::.:;'-;''::
:-X':-.-
:;:>
;''|;';|
': >::::
<:,:: :'.\-..>
--.;-;>:: :.:- v
"^*S**:
; :': :-'::
PRESSURE DROP ACROSS CARBON = 20.38 INCHES H20
PRESSURE DROP ACROSS PLATES = 10.19 INCHES h20
TOTAL PRESSURE DROP ACRCSS STAGES = 30.57 INCHES H20
192
-------
S02 SORBER DESIGN
RUN NUMBER TEST-19 DATE 7 27 71
TOTAL CARBON RATE = 50._640_LBS/HR_ _ _ _
OUTLET CARBON i TOADTNG "= 0.18375 LBS ACT07FB"*"CARBON
HtlGHT OF CARBON/STAGE = 9.00 INCHES
PIAAET_?.? °.f. VESSEL = IB. 0 INCHES _____
""S'EO"=""~ " 0. ~~"
TOTAL GAS FLOW RATE = 18969. 5CFH
INLET S02 CONCENTRATION = 2000. PPM
INLET NO CONCENTRATION = 150. PPM
INLET 02 VOLUME FRACTION = 0.0460 ^ .: : . ,. ,: . . ;;
INLET H20 VCLUME FRACTJ CN = 0.1000 :;;^ ,_;:;,. \..^_ ,
"OUTLET"S02" CbNCENtRAYlON = 200." PPM
_I?M.p.f?*iyM. '= 200.0 DEC. _F
S02""CO'NC"ENtR"ATION. ACIOTOADTNG "
STAGE PPM LBS ACID/LB CARBON
..__._._ i'y.ii::y:!.:,,, . :;V;V; 2000. l:^":1- ' 0 !837__ . ..
2 1586. .671413
3 1136. 0.0952
4 680. 0.0486
'.275. :£:y%j^£^%;:&.,.,.;.c
-TQJ.A.i .PA_R._60N REQUIRED - 46.94 INCHES n
: TYOTAL "STAGEST REQUIRED... ASSUMING^ aOJ^CHES^
L^SPACE. VELOCI TV.. « 2744<'ffiHRj^
PRESSURE DRCP ACROSS CARBON = 23.47 INCHES H20
PRESSURE DROP ACROSS PLATES_= I K73_ INCHES H20 . _ _
f TOTAL PRESSUR'E"DROP"rAC"RdSS" STAGes"=.;i. 35,20 INCHES ;H20 : :v
193
-------
S02 SORBER DESIGN
HUN NUMBER
TEST-20 DATE 7 27 71
TOTAL CARBON RATE = 50.64_0_LHS/HR
"OUT L C T C A R B ON U6 A f) ING" = " O . l"8 3 7 5" L B S A CI 0 / L 8 C A~RB 0 N"
HiflGHT OF CARBON/STAGE = 9.00 INCHES :. .
DIAMETER OF VESSEL = 1_8.0 INCHES, .,...;.-. ^...^4\---t''\
CARBON USL:l)"= 0.""
TIITAL GAS f:LOW RATE = 18969. SCFH
INLET SC2 CONCTNTRATION = 2000. PPM
'INLLT NO CGNCENTRAI IUN = " Tf->6.~
INLET 02 VOLUME FRACTION = 0.0460
INLET H20 VCLUME FRACT I CN_=_ 0.1 f>00
OUTLET S02" CO.NCENTRAT ION -"
"PPM
200. "PPM
TEMPERATURF. =200.0 DEG._F _
"~Sb2""CONClENTRAT'lON'"
STAGE PPM
2
3
_
0.21
_
1452.
856.
__ 302_.
200.0001;
ACID LOADING
L8S ACIO/L8 CARBON
0.1837 _
"071277"
0.0665
O._0098
"0.0 "
TOTAL CARBON REQUIRED = 37.93 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE
= 4.21
SPACE VELOCITY =
3396. l/HR
PRESSURE DROP ACROSS CARBON = 18.97
PRESSURE DROP ACROSS PLATES = 9.48
TOTAL PRESSURE DROP ACROSS STAGES =
INCHES H20
INCHES H20
28.45 INCHES
H20
194
-------
S02 SCRBER DESIGN
RUN NUMBER TEST-21 DATE 7 27 71
TOTAL CARBON RATE = 50.640 LBS/HR
OUTLE T""CARBON LOADING "*""b7llT375TBS""A'CTD7rB'~'C'AR'BON"
HEIGHT OF CARBON/STAGE = 9.00 INCHES'": :. ,
DIAMETER OF VESSEL = 18_.J)_ INCJHEJJV^ _ '^^^ ^ . ;:-':
CARBON USED" =~Cf.~" " '~~^~ ~
TOTAL GAS FLOW R-ATE-= 18969. SCFH
INLET S02 CCNCENTRATION_=__ ,___ 2000. PPM
J'NLE T :NQ':TONC t-NTR AT i ONT =~V~ - A so".;
INLtT 02 VOLUME FRACTION*^ :'!ol0460' :":-".
INLET H20 VCLUMb FRACTION = ,0.20pp_ _
CUTLET SW CONCENTRATION "= ' "200V PPM
V . | i
STAGED
2
3
0,66
i.E ='20Q;o DEC. F
j |/I T ',*'' ~
' : "' PPM
1335.
618.
200.0001
i .. '.: '" rMu! I!.-.
ACID LOADING T
v LBS ACID/LB CARBON ; : r;:.
0. 1837 ' C :
. 0.1156
0.0422
0.0
"TOTAL "CARBON REQUIRED = 32.90 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 3.66
SPACE VELOCITY = " ;. 39T5^"l/HR
JPRESSURE CROP ACROSS CARBON =; 16.45 INCHES H20
PRESSURE DROP 'ACROSS "PLATES' = 8.23 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES = *24.68 INCHES H20
195
-------
APPENDIX A-9-5
EFFECT OF THE INLET S0£ CONCENTRATION ON THE TOTAL
CARBON BED DEPTH REQUIRED FOR 90% REMOVAL
197
-------
S02 SORBER DESIGN
RUN NUMBER TEST-35 DATE 7 27 71
__TOTAL CARBON RATE = 12.690 LBS/HR
OUTLET CARBO~N LOADING = 0.10375 LBS ACID/LB CARBON
HEIGHT IJF CARBON/STAGE - 9.00 INCHES
DIAMETER OF VESSEL * 18.0 INCHES _ ...
"CARBON USED - o.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION = 500. PPM
INLbT NO CONCENTRATION = " 150. PPM " "
INLET 02 VOLUME FRACTION * 0.0460
INLET 1120 VOLUME: FRACTION = .0.1300
'OUTLET S02 CONCENTRATION = bo. PPM
_TEMPERATURE = .200.0. DEC.. F
STAGE
1
2
0.69
S.02 CONCENTRATION
PPM
500.
237-
50.0000
ACIO LOADING
LBS ACID/LB CARBON
_ . 0.1837 .
0.0761
0.0
TOTA1, CAHPON RF.QUI.RED * 2.4.23 INCHES .
"TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 2.69
_S.PACE ..VELOCJ.IV._= 5.3_16_._L/HR
PRESSURE DROP ACROSS CARBON = 12.12 INCHES H20
_PReSSUR.E_URtJP_.ACR.Q.SS.P_LAT_ES._5 &._06_JJ-JC_H.E5_H2_q
TOTAL PRESSURE DROP ACROSS STAGES = 18.17 INCHES H20
RATE EXPRESSION USED IN DESIGN CALCULATIONS
RATECIII=COEFF * (1-X(I)/XS)**A * (YS02**BI * (V02**C) * (YH20**D)
WHERE COEFF-K * EXPI-E/R*(II iT*460)))
T= 200. XS= 0.38 Y02= 0.046 YH20* 0.130
-E/R" 5520. A= 1.000 B= 0.400 C= 0.630 U= 0.730
_.K"0.000159 _..._._ .. __ _.._ .,_ _
198
-------
S02 SCRBER DESIGN
RUN NUMBtR TEST-36 DATE 7 27 70
jr.U.T.AL.CARHON._RATE = 25..380 ..LRS/HR . .
OUTLET CARHON LOADING = 0.13375 LUS ACIl)/l."(J"CARBON
HEIGHT (IF CARBON/STAGE = 9.00 INCHES
..DIAfETER (^ .VESSEL..1. l.8.Q...HCt.CS
CARBON USED - 0.
TOTAL CAS FLOW RATE = 18069. .SCFH
_LNLE.J_S02._CP_N.C.F.MKATinN... = looo., .PP.KL
INLET NO CONCENTRATION » 150. PPM
INLET 02 VOLUME FRACTION « 0.0460
.INLET. H2C) VOLUME FRACTION =. ..Q. U00_
OUTLET S02 CONCENTRATION * 100. PPM
_JtMPLRATUKt V?00.0 DEC. F
S02 CONCENTRATION ACID LOADING
STAGE PPM IBS ACID/LB CARBON
. ... .1 1000. OL,.W7._
2 635. 0.1092
3 247- 0.0299
0.43 LOO..OOOQ 0,.0,..__
TOTAL CARBON REQUIRED = 30.84 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE * 3.43
SPACE VELOCITY * 4177. l/HR :
ppp$«;iipp [,qnP ACROSS CARBON ." 15.42 INCHES H20
PRESSURE DROP ACROSS "LATES ' 7.71 INCHES H/ll
TOTAL PRESSURE DROP ACROSS STAGES = 23.13 INCHES H20
;. EXPJxnss.lON-USED-.JtJ.
RATECII)«COEFF * U-XII )/XS) **A * =- 0.130....
K«0.000159
199
-------
S02 SORBER DESIGN
RUN NUMBER TEST-37 DATE 7 27 71
TOTAL CARI10N RATE = 38.060 LBS/HR
"dilUt-T CARBON "LOADING = 0.18375 UBS ACID/IB CARBON
HEIGHT UF CARBON/STAGE = 9.00 INCHES
uIAKETER OF VESSEL '- 18.0 INCHES. _._..
"CARBON USED = 0.
TOTAL GAS FLOW RATC = 18969. .SCFH
INLET S(!2 CONCENTRATION = 1500. PPM
"INIET'NO CONCENTRATION = 150. PPM
INLET 02 VOLUME I'KACTION = 0.0460
INLET H2(l VC.LUME FRACTION f 0_.1300 _
"OUTLET so2 CONCENTRATION = it>o. PPM
TEMPfcKATUKE « 200.0 DEG. F
S02 "CONCtNlRAI ION ACID LOAUING
SlAGt PPM LBS ACiO/LB CARBON
1 1?>00. _ 0. 1837
I 1062. 0.12'.l
3 587. 0.0092
i\ J63._ _ _ _p_.00i5
0.03 150.0001 0.0
TOTAL CAROON REOUIREO = 36.31 INCHES
-JfllAL S J ACE S_REQU J.KEO_ASS_UMlN.G_9_._eO \ NCH£$_..C_ARBON./ SI AG.C__r_..'s_._03 ,
SPACE VELOCITY = 3547. 1/HR . : '
PRESSURE DROP ACROSS PLATES = 9.OB INCHES H20
J.Q.TAU._PRESSURE._DRp.P. ACROSS.3JA6Ei.«_ _2J_li4_IN£H£S..H2a
RATE EXPRESSION USED IN DESIGN CALCULATIONS
..RATECU ) = COEFF * (l.-X( I )/XS.).**A * (ySD2**B) * (V02**C) * (YH2q**D).
KHCRE COEFF = K » EXPI -E/R*t I/(T + 460)))
.. .. T= .. 200. .. _ X3= 0..38 _...y02= .. 0,046. YH20=. ,._O.J30
-F/R= 5520. A= 1.000 B= 0.400 C= 0.630 0= 0.730
K-0.000159
200
-------
S02 SORBER DESIGN
RUN NUMBER TEST-38 DATE 7 27 71
_T.PTAL CARBON. RATF = 50..75Q LOS/MR _
OUTLET CARBON LOADING = 0.18375. LttS~AC.1 "b/LB~ CARBON"
HEIGHT OF CARBON/STAGE = 9.00 INCHES
_P1AMF.TF.R. OF..VESSFL *_ l8.0_LNCJiF.S
CARBON USED - 0.
TOTAL GAS FLOW RATF: = 18969. SCFH
IN'l.ET_SP2 CONCENTRATION = _ 2000. PPM
INLET NO CONCENTRATION = 150. PI>M
INLET 02 VOLUME FRACTION = 0.0160
_..)_NLET .H2Q .VG.LUME FP ACT.I ON _?.__Q, 1 300
OUTLET S02 CONCENTRATION - 200.' PPM
_!Er,PERATURF:. '...200.0 DEC. F
S02 CONCENTRATION ACIO LOADING
STAGE PPK UBS ACIU/LB CARDON
I ..2000.. ..__._. Q.1HJ7
2 1504. 0.1330
3 962. 0.0777
A
-------
S02 SORBER DESIGN
RUN NUMBER TEST-39 DATE 7 27 71
TOTAL CARBON RATE = 63.440 LBS/HR . .
"CUTLET CARBON LOADING » o.13375 LBS ACID/LB CARBON
HEIGHT OF CARBON/STAGE « 9.00 INCHES
DIAMETER OF VESSEL = IB.p INCHES _
"CARBON USED = o.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION =_ _ 2500. PPM
INLET NO CONCENTRATION = 150. PPM
INLET 02 VOLUMF FRACTION * 0.0460
INLET H2H VOLUME FRACTION « 0.1300
"CUTLET su2 CONCENTRATION = 250. PPM
TEMPERATURE = 200.0 DEC. F
S02 CONCENTRATION AC IU LOADING
STAGE PPM LBS ACIO/LB CARBON
1 ._ 2500. . _ . _..... .P..J.837..
2 1953. 0.1391
3 1358. 0.0904
4 _ _ ?62.. Q.041.7
5 253. 0.0000
0.01 249.9999 0.0
.TOTAL CARBON PFOUIREO « _ 45.01 INCHES
TOTAL STAGES K( QUIRED A'SSUMING 9.00 INCHES CARBON/STAGE = 5.01
SPACF VELOCITY 2ft5.8.t_JL/t
PRESSURE DROP ACROSS CARBON = 22.53 INCHES H20
.PRESSURE DROP ACROSS PLATES.. = l.U27_J NCHE.S...H2.0
TOTAL PRESSURE OftOP ACROSS STAGES = 33.80 INCHES H20
RATE EXPRESSION USED IN DESIGN CALCULATIONS
SATECI I I^COEFF * t I.-X( 1 )/XS)**A * (YS02**B) * (Y02**C) * (YH20**D)
WHERE COEFF = K * EXPI-E/R* ( \l ( T+'t60 I I I
T* 200. XS= 0.38 Y02= 0.046 YH20= 0.130
-E/R* 5520. A= 1.000 B« 0.400 C= 0.630 D= 0.730
K=0.000159
202
-------
S02 SDRBER DESIGN
RUN NUMBER TEST-40 DATE 7 27 71
_J.QtAL. CARBON. RA1E...T...76. 130 L.BS/HR ____ ___
OUTLET CARBON LtJAUING = 0.18375 LBS Aclu/LO CARBON""
HEIGHT OF CAKbON/STAGE « 9.00 INCHES
i_U.l.A^£.TfH. Qf-VE.SSE.L._«._1.8..0-IMCHES ____
CARBON USEO =0. __
TOTAL GAS FLOW RATE = 18969.' SCFH
_lN.L,tJ_.S02_C-a/K.E.MLR-AT.LOM..r _______ JflQQ. PPM __ ____
: INLET NO' CONCENTRATION = 150. PPM
JNIET 02 VOLUME FRACTION * 0.0460
L_lI4LEt_H20. VOLUME. FRACT.10N_.= __Q._l_3iiD ___ ____
OUTLET S02 CONCENTRATION = 300. PPM
_J.EMPERATURE =_200,Q OEG, .F ____________ . _____ _______ ._
S02 CONCEN1RATION ACID LOAOJNG
STAGE CPM LBS ACID/LB CARBON
_______ ..... 1 _________ .JOOO. ____________________ .O.L8J.7
2 2409. 0.1435
3 1768. 0.0998
.a «
5 316. O.OU5
0.42 300.0000 0.0
TOTtl r.ARRIlN RFQtltRFn = 48. 78 IMf.HF!;
; TOTAL STAGES REQUIRED ASSUMING 9.00 INCHtS CARBON/STAGE = 5.42 :.-: : , :
_.SAAC£ -VEI.OCI TJf_=__
PRESSURE DROP ACROSS CARBON » 24.39 INCHES W
TOTAL PRESSURE DROP ACROSS STAGES = 36.59 INCHES H20
$. ,- -, - *'.; .»>.. .: - -- " ^*; -y^j^k'^
RATE EXPRESSION USEO IN DESIGN CALCULATIONS
*ATECU»=COEFF * ( l~K( I )/XS)**A *
-------
S02 SORBER DESIGN
RUN NUMBER TEST-41 DATE 7 27 71
_TOTAL CARBON.RATE =101. 500 . IBS/MR . _ ___..
OUTLET CARBGN LOADING = 0.18375 LUS ACID/LD CARBON
HEIGHT OF CARBON/STAGE = 9.00 INCHES
_DIAMF.THR OH VESSEL = 18.0. INCHES.
CARBON USED * 6.
TOTAL GAS FLOW RATC = 10969. SCFH
_ INLET S02 CONCENTRATION «_ _4QOC). PPM __
INLCT NO CONCENTRATION = 150. PPM
INLET 02 VOLUME FRACTION = 0.0'<60
INLET H20 VOLUME FRACTION ?_ .0.1300
OUTLET SU2 CONCENTRATION = 400. PPM
_TEMPFRATURE = 200.0 DEC-. F _ . ._. .
S02 CONCENTRATION ACID LOADING
STAGE PPM IBS ACID/LB CARDON
_ 1 4000. _ 0.. 1837 ..
2 3332. 0.1496
3 2612. 0.1128
_ 4 1867. 0.0747
5 1143. 0.0377
6 510. 0.0054
.0...2Q 4QQ nO.QO.0. J3,0
TOTAL CARBON REQUIRED = 55.79 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 6.20
SPACE VELOCITY = 230<3, 1/HR
_RRESSURE .DROP. ACROSS..CA.RBON -: ?.7.9D_IilCHESi_H2D
PRESSURE DROP ACROSS PLATES '- !.3.95 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES * 41.84 INCHES H20
..RATE.JXPRCSS10N USEQ..JN -DESIGN CALC.ULAT.IONS.
RATECII)=COEFF * (1-XII)/XS)**A * (YS02**B) * (Y02**CI *
-------
APPENDIX A-9-6
EFFECT OF THE INLET SC>2 CONCENTRATION ON THE TOTAL
CARBON BED DEPTH REQUIRED TO ACHIEVE AN
OUTLET S02 CONCENTRATION OF 100 PPM
205
-------
$02 SCROER DESIGN
RUN NUMBtR TEST-36 DATE 7 27 70
_TDL4J._£ AR BON...R 4 T E. ..= .2_5_.J 8 0_Lfl SZHR_
OUTLET CARBON LOADING « 0.18375 LBS ACID/LB CARBON
HEIGHT (IF CARBON/STAGE = 9.00 INCHES
CARBON USED = 0.
TOTAL GAS FLOW RATE = 18969. .SCFH
INLET SQ2 CONCENTRATION,* 1.00
-------
S02 SURBER DESIGN
RUN NUMBER TEST-49 DATE 7 27 71
JLOT.AL CARBON. .RATF =03.570 LBS/HR
CUTLET CARBON LOADING = 0.18375 LBSACID/LB CARBON
HEIGHT OF CARBON/STAGE = 9.00 INCHES
OJAHETER OF VESSEL _= 18.0 INCHES_
"CARBON USED ^ o.
TOTAL GAS FLOW RATE = 18969. SCFH
_INLET SQii CONCENTRATION .5 _ 2000. PPM
"INLET NO CONCENTRATION '= "I"*O"."PPM"" " " "~
INLET 02 VOLUME FRACTION - 0.0460
INLET H20 VOLUME FRACTION * 0.1300 _
OUTLET S02 CONCENTRATION - lOO.Vf'M
TtMCtRATURL = 200.0 OEG. F
S02 CONCENTRATION ACIOLOAOIHC"
STAGE PPM LBS ACIU/L8 CARBON
1 2000, _ Q.l(!37
2 liO-V, 6.13^7
3 968. 0.0838
A 451. _ Q.Q338
"O.B« "166.0060 6.6
TOTAL CARBON RFQUIRFO = 43.90 INCHES
__TQTAL_S.TAGES. REQU IReO_ ASS.UM I NG. 5, .OJJ..I NCHE.5._ CARBON/ STAGE _=__4.88__
SPACE VELOCITY = 2934. I/HP.
PRESSURfc UKUP ACROSS CARbOH = 21.95 INCHES H20
PRESSURE DROP ACROSS PLATES = 10.98 INCHES H20
_TOTAL_PRESSURE DROP ACROSS STAGES_= J2.93_INCJ1ES_H20__
RATE EXPRESSION USED IN OESIGN CALCULATIONS
l )=COEFF * (1-XI1 1/XSI**A *_ ( YS_C2**B I. * _ I Y02**C ) *._LYH2a**PJ.
hHERE COEFF=K * EXPt-E/R*(I/(T+460)))
T= 200. XS= 0.38 Y02= 0.0'.6_ ._ YK2P5... 0.110 _
-E/R= 5520. A= 1.000 B= 0.400 C» 0.630 0= 0.730
K=0.000159
207
-------
S02 SORBER DESIGN
RUN NUMBER TEST-50 DATE 7 27 71
_TOTAL CARBON.RAU = 11Q..OOO LRS/HR
OUTLET C AC, II ON LOADING = 0.18375 LHS ACIU/LB CARBON
HEIGHT Or CAROON/STAGE -' 9.00 INCHES
OlAMEH* uf VESSFl,_=L IB.Q INCHSi. ____________ __
CARIHJU USED - 0.
TOTAL GAS FLOW RATF = 18969. SCFH
INLI 1 SO? COUCrNTP.AT10N_=. .4000. ..P.PM ____________________
INLET NO CONCfcNfUATlhN "= 150. PPh
INLET 02 VOLUME FKACT10N = 0.0460
INLET ll^O VO.LUMb FRACT[ON. = ___O.UOO.__. ____________ . _______
OUILEI S02 CONCENTRATION - 100. PPM
E MATURE =.200.0 DfG. f ..... ____ .._ ....... _ ....... .
SC12 CONCENTRATION ACID LOADING
STAGt PPM LBS ACIU/Lli CAkOON
1 ... . .3000., ....... __________ ...... 0..1837 ......
2 3332. 0.1523
3 2620. 0.1187
..'t .. 186"?, ______ ___ ...... _______ 0.08
-------
APPENDIX A-9-7
EFFECT OF THE INLET SC>2 CONCENTRATION ON THE TOTAL
CARBON BED DEPTH REQUIRED TO ACHIEVE AN OUTLET
S02 CONCENTRATION OF 50 PPM
209
-------
S02 SORBER DESIGN
RUN NUMBER TEST-35 DATE 7 27 71
_LPTAL CARBON RATE = 12.69Q.L6S/HR
__ .
r OUTLET CARBOli LOAUING = 0.18375 LBS ACIO/LB CARBON .'
i HEIGHT UF CARBON/STAGE » 9.00 INCHES . i . - '.
LPJAMETER OF_V£SSEL_=_ la.q INCHES ___ ' ":. .-.. -'"}.
CARBON USED « 0.
TOTAL GAS FLOW RATE = 18969. SCFH
_1NLET S02 CONCENTRATION = 500. PPM
f: iwit'i NO CONCENTR'ATION' =~ "isb. PPM
I. INLET 02 VOLUME FRACTION « o.04&o
L.INIE.T H20 VOLUME FRACTION = Q._130.Q
OUTLET SO? CONCENTRATION « i6. PPM
TEMPERATURE - 200.0 DEC. f
£.'v ':. STAGE
1
2
0.69
S02 CONCENTRATION
PPM
500.
237.
50.0000
ACID LOADING ;i ; .;: -
>'LBS ACID/LB CARBON, '';. '. "'' , i-;' -' . -'?... : s . ;. , . ''.?.'" : >
0.1837 :.. ! ."..
0.0761
0.0
CARBON_RE9UI.REO = __ 24. 23_ INCHES.
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 2.69
_iPA.QE VELOCITY = 5316. 1/HR
PRESSURE OROP ACROSS CARBON » 12.12 INCHES H20
/PRESSURE DROP ACROSS PLATES = 6.06 INCHES H20
IUIAL KKtSiUkt DROP ACROSS STAGES = 18.17 INCHES H20
I-: :: RATE EXPRESSION USED IN DESIGN CALCULATIONS
RATECU ) = COEFF * Il-X (I I/XS)**A * (YS02**B) * (Y02**C) * (YH20**D)
WHERE COEFF-K » EXP(-E/R*(I/IT+460)))
T« 200. XS* 0.38 Y02« 0.046 YH20«= 0.130
-E/R* 5520. A» 1.000 B- 0.400 C« 0.630 0» 0.730
_.K-0.000159. , , '. L. .
210
-------
S02 SI1KBER DESIGN
RUN NUHHFR TFST-'jl OATP 7 27 71
TOTAL CARBON RATf = 5" 1 Ysu2**o"r * (Y02*'*cT~*"TYH2ov*br
WHtRH CUEFF'K * EXP(-E/«*I 1/(T+'.601 I I
I> 200.
-E/R« 5520.
K'O.000109
'67Ja"
i.ooo
Y02"
B=
0.046
0.400
"YH26-
C-
0.130
0.630
0.730
211
-------
S02 SORBER DESIGN
RUN NUMBER TEST-04 DATE 7 27 71
_J£TAL CARBON RATC *lll«.4PO LBSVHR
OUTLET CARRON LOADING = 0.18375 IBS ACID/IB CARBON
HtlGMT OF C.ARBCJN/STAGC = 9.00 INCHES
_PIAMCUK OF. VfSSEL...!L.18.«.D_LMCJi£i__
CARBCN USfcU = 0.
TOTAL GAS FLOW RATE = 18969. SCFH
1 .NLE 1_ .S.O.Z. ..C.ON.C.E NT P. AT_.LO.N_= A 0_00._ P P.M
INLET HU CONCENTRATION = 150. PPM
INLET O/ VClUf-r FRACTION * 0.0460
VOLUME F.RAC.T1QN_* ._0,JJQP_
CUTLET SU2 CONCENTRATION = 50. PPM
JEMPCRATUKt = 200.0 DEC. F _..
S02 CONCENTRATION AC I 0 LOAOJNG
STAGE PPM IBS AC10/LB CARBON
. 1 . .__ 4000. _ Q.1837_
2 3332. 0.1527
3 2621. 0.1195
_...... Jt ... ...-'-. 1893, , ..0.0656... ...
5 HUB. 0.0528
6 ' 567. 0.0239
_I 115. Q.QD.Sfl
0.25. -50.0000 0.0
TOTAL CARBON RFQUIP.ED = 65.21 INCHES
._TOTA( MAUI-S RbUUIRfcO AS!>UnlNL. 5520. A« 1.000 B« O.'iOO C= 0.630 0= 0.730
K=0. 000159
212
-------
APPENDIX A-9-8
EFFECT OF THE OUTLET H2S04 LOADING ON CARBON ON THE
TOTAL CARBON BED DEPTH REQUIRED TO REMOVE 90% '
OF AN INLET S02 CONCENTRATION OF 2000 PPM
213
-------
S02 SORBER DESIGN
RUN NUMBER TEST-7 DATE 7 27 71
TOTAL CARBON RATE = 50.640 LBS/HR
["OUTLET CARBON" LOADING = 0.1837.5 LUS AC ID/LB~CARBON
i HEIGHT OF CARBON/STAGE =
I DIAMETER OF VESSEL =
_
CARBON USED = 0.
TOTAL GAS FLOW RATE = 18969. SCFH
JNLET S02 CGNCfrNTRATlQN_j= 2000^ PPH
TNYETWO~TONCENTRATlON = :,, 150~7 .
INLET 02 VOLUME FRACTION = '0.0460
INLET '20VCLUME FRACT I CN ~ 0.
OUTLET S02 CONCENTRATION = 200. PPM
TEMPERATURE = 200.0 DEC. F
< - STAGE
^ 1
2
3
S02 CONCENTRATION
PPM
2000.
1504.
962.
438.
,ACID LOADING ,,;%: -:,.^^f, + .- . .
LBS AC 1 D/LB C ARBON ^f^fe^;' .'.;
0.1837 ,^:s::yUSil? ^A?- ; /
0.1329
0.0774
0.0237
TOTAL CARBON REQUIRED = 40.76 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 4.53
|: SPACE VELCCITY.,=;;;;;4:g3i:61r;^
:I:S?^^*^as;'
PRESSURE DROP ACROSS CARBON - 20.38 INCHES H20
PRESSURE ORRP ACROSS PLATES = 10.19 INCHES H20
TOTAL PRESSURE DROP ACRCSS STAGES = 30.57 INCHES H20
214
-------
S02 SORBER DESIGN
RUN NUMBER TEST-16 DATE 7 27 71
TOTAL CARBON RATE = .50_^40_ L__BS/HR
"OUTLET cARBONToADiNG = o.oTrel LBS ACro7lT~cAR'BON"
HEIGHT OF CARBON/STAGE = 9.00 INCHES
DIAMETER OF VESSEL = 18j.O__I_NCHES ____
"CARBON usED"-^ cT. " ^ '' ' ""
TOTAL GAS FLOW RATF = 18969. SCFH
INLET S02 CONCENTRATION =_ 2000._PPM
INLET NO CONCENTRATION"^"" """ ~II>O.~P"£H~~:':. ~
INLET 02 VOLUME FRACTION = 0.0460 :: : :
INLET H20 VLLUME FRAC.] I CN_f___p_._l_300 ___
OUTLET" so2 coNCENTRAnoN = 200". PPM"
TEMPERATyRE = 2.00.0 DEG_._F
"r'sdY""CONCENTRATION " ACID LOA'D'ING
: STAGE:; . PPM . LBS ,ACl D/LB CARBON
2000. 0.0919
2 1291. 0.0192
3 588. 0.0
0.75 200.0001 0.0
TOTAL CARBON REQUIRED = 33.76 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE - 3.75
r"TpATEnin!UbciTY^ ,:, -rii^^^C^
? PRESSURE DRpP_ACRgSS CARBON V\: 16;88 INCHES H20 ::'.'' ^Lj^LJ-;.::?'
""'PRESSUR'E "DROP ACROSS'TLAT'ES = " a"."^4 INCHES""H2"o"
TOTAL PRESSURE DROP ACROSS STAGES = 25.32 INCHES H20
215
-------
S02 SORBER DESIGN
RUN NUMBER
TEST-17 DATE 7 27 71
TOTAL CARBON RATE = 50-640 LBS/HR
OUTLET "CARBON LOADTNG"'= 0". 27"562 WS "AC I DTOTTlARBON
HtlGHT OF CARBON/STAGE = 9.00 INCHES " i:. ;:v.. v. :J :;
_DUMETF:R OF VESSEJ. = _18.0 INCHES ^JlIilMliS^-'^
CARBON "USfcD"=""" ~ 0.
TOTAL GAS FLOW RATE = 18969. SCFH
INLET S02 CONCENTRATION = _ 2000. PPM_ __
INLET NO CONCENTRATION'-- " TSO.'PPNT" ;'---
INI.ET 02 VOLUME FRACTION ~ O.OA60 A',.
INLET H20 VCLUME FRACTICN =__0^1300 _^_ ; _
OUTlET SU2"CCNCCN'TKATfUN""-""" "200. "P'PM
TEMPERATURE = 200.0 DEC. F
"502 CONCENTRATION
STAGE
__
5
0.32
:PPM
,. 2000
"ACID LOADING
LBS ACID/LB CARBON
0.2/56 :...;'
1409.
_
665.
0.2't79
0.2151
0.1780
1388
1019
200.0001
0.
0.
0.0912
TOTAL CARBON REQUIRED = ; 56.90 INCHES
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE-^ 6.32
SPACE VELOCITY =
2264. 1/HR
PRESSURE DROP ACROSS_CARBCN = _28_.45 J_NCHES H20 __
"PRESSURE DROP" ACROSS "PLATES'^ "14.22 INCHES "H2o"
TOTAL PRESSURE DROP ACROSS STAGES = 42.67 INCHES H20
216
-------
S02 SOR8ER DESIGN
RUN NUMBER TEST-18 DATE 7 27 71
JJ?TAk CARBO_N RATE = 50.640 LBS/HR
CUUETCA~RBCN 'LOADTNG" = 0%3675~0 LBS~ ACTD/TF
HEIGHT OF CARBON/STAGE = 9.00 INCHES
DIAMETER QF yESSEL = 18.0 INCHES
"CARBON'USED~ = '"
CARBON
0.
TOTAL
INLET
"INLET
INLET
INLET
OUTLET
PPM
GAS FLOW RATE = 18969. SCFH
S02 CONCENTRATIONI _= _200p. PPM
NO CONCENTRATION"^ " "156".
02 VOLUME FRACTION = 0.0460
H 20 VOLUME F R ACT! ON - 0_._l 3 0 0_
S02" CONCENTRATION = " "
200. PPM
TEMPERATURE = 200.0 OEG._F _
"S"02 CONCENTR AT ION
STAGE PPM
l.:'.-:'-.-:'"V- . - 2000. 'T
ACTt5 LOAOTNG" "
LBS ACID/LB CARBON
; 0.3675
2
3
4
5
6
/
8
9
10
n
12
13
14
0.38
1967.
1925.
1872.
1806. .,«
'1723. "3 \
1 622.+. T^
1498.
1348.
1173.
970.. -vx
7 4 6. ';;£
510. :?
281.
200.0001
0.3641
0.3598
0.3544
^.::f:.:*.:-..?,i*;.:^.:-.<.. 0.3476 , .: :-/: ;..
;:::;>i:M:ii::;i..tr^,:::.::iC:v:r:,v.:i.o ^^qi ' ..;:> ;-:- ;--r. ":
-.;. .v.;.::::v:*'f .?:..'. T;V,:, -Af-:.:, .', U * * * J L : - '. - .-..,
^^^^'^^}:-'- 0.3281 :'. '..: . ;=::
0.3160
0.3008
0.2827
'^:::,K^-m'(<:m^----: ' ;.; 0.2620
^i^liJiitiiSW'f :i';-:-' 0. 2390
::;::t^!Nv|!|5-:;;i:;:^?::::l:', 0.2143
0.1914
0.1831
JOTAL CARBON R F_Q UIR iD _=_ _ ili*:38 I NCHESl . ,
TOT'AL"S"TAGES"REQUTRED~ASSUMING 9.00 INCHES CARBON/STAGC =14.38
SPACE VELOCITY =
996. 1/HR
PRESSURE DROP ACROSS CARBON = 64.69 INCHES H20
_PRESSURE DRCP ACROSS P_LATES _=_ _32 ._34_JNCHES H20
TOTAL PRESSURE DROP ACROST STAGES = 97.03 INCHES H20
217
-------
APPENDIX A-9-9
EFFECT OF THE TEMPERATURE ON THE TOTAL CARBON BED DEPTH
REQUIRED TO REMOVE 90% OF AN INLET S02 CONCENTRATION
OF 2000 PPM
218
-------
S02 SORBER DESIGN
RUN NUMBER TEST-7 DATE 7 27 71
TOTAL CARBON RATE =_
"OUTL'ET" C "ARBOirLOAD ING
HEIGHT OF CARBON/STAGE =
_DIAH E1ER_OF_VESSEL = 18.0
CARBON "US ED" =
TOTAL GAS
S02
"NO""
50JL640J.BS/HR
= . 0."1837.5
LBS ACt.D/LB CARBON"
:9.00 INCHES.
INCHES
JNLET
INLET
INLET
INLET
"OUTLET
o.
FLOW RATE = 18969. SCFH
CGNCENTRATION_f_ 2000. PPM
CONCENTRATTON = .:,, 150. PPM"
02 'VOLUME
FRACTION =
P R ACT I CN =
150
: 0.0460 v
:;,0 . 1 300
S02 CONCENTRAlON =
200. PP'M
_= 200 <._^
S02"CONCENfRAflON
, STAGE
; i
2
3
PPM
2000.
1504.
962.
438.
LBS ACIP/LB CARBON
0. 1329
0.0774
0.0237
^2 00,000 i::,
0.0
TOTAL CARBON REQUIRED = 40.76 .INCHES
TOTAL STAGES REQUIRED ASSUMING 9,00 INCHES CARBON/STAGE = 4,
53
SPACE VELOCITY =
3161. 1/HR
PRESSURE DROP ACROSS CARBON = 20.38 INCHES H20
PRESSURE DROP ACROSS PLATES - 10.19 INCHES H20
TOTAL PRESSURE DROP ACRCSS STAGES = 30.57 INCHES H20
219
-------
S02 SORDER DESIGN
RUN NUMBER TEST-22 DATE 7 27 71
TOTAL CARBON RATE = 48.790 LBS/HR
OUTLET CARBCN LOADING = 0.18375 LBS ACID/LB CARBON
HEIGHT OF CARBON/STAGE = 9.00 INCHES
_OIAMETCR OF VESSEL = 18.0.. INCHES .; -v -:::;;;.''::; <-v:: ^__
CARBON USEO~=0.
TOTAL GAS FLOW RATE = 18276. SCFH
INLET S02 CCNCENTRATIO_N_= _ __200_0_._ PPM
INLET NO CONCENTRATION "-" " TSO". PPM~ " ."."
INLET 02 VOLUME FRACTION = 0.0460 .< . ;
INLFT H20_ VOLUME FRACTION - 0. 1300 '''''"'.
OUTLET s"02 "CCNCENTRATION"^" 2601 "PPM"
STAGE
1
2
3
4
5
0.52
S02 CONCENTRATION
.PPM - ".. : ,:;.
. ..'.:;, . 2000. i. i .
1615.
1198.
771.
376.
200 . GOO 1
ACID LOADING
-. LBS ACID/LB CARBON A :*
.:;i:;::.:-'-;".;:'::-'.. :: 0.1837 /:\,":^^:
0.1443
0.1016
0.0579
0.0174
/* rs
w * o
CARBON_ _
"TOTAL"STAGE'S "REQUIRED. ASSUMING 9".oo""iNcvrE"sT'CARBON/sTAGF;= 5T52
SPACE VELOCITY = 2498.:1/HR:
PRESSURE DROP ACROSS CARBON = 24.84 INCHES H20
PRESSURE DROP ACROSS PLATES =_ _L2'42 INCHES H20
TOTAL PRESSURE DROP ACROSS" STAGES ="'T 37.27" INCHES ~H2lf
220
-------
S02 SCRBER DESIGN
RUN NUMBER TEST-23 DATE 7 27 71
TOTAL CARBON RATE = 47.070 LBS/HR
OUTLET "CARBON LOAD I N(T ="'OVl 8375~niT"^CTiJ7rB~C"7rRBON'
HEIGHT OF CARBON/STAGF. = 9.00 INCHES
DIAMETER OF VESSEL =_l_8_.0 INCHES ::
CARBON USED = 0. '" ~ ~
TOTAL GAS FLOW RATE = 17633. SCFH
INLI-T SG2 _CCNCENTRATION =_ 2000_. PPM
"INLF. T NG~'CONCENTRAT ION "=" T50- ~"PPM""""~~":~"
INLET 02 VOLUME FRACTION = 0.0460 '.:-.--.''x '' ::'^^\
INLET H20 VOLUME '-RACTICN_^ 9_«J._300 :;;..: . :..':^:.:.;-
"OUTLET S02" CONCENTRATION"^ 200T"PPM -^ :-
TEMPERATURE
| STAGE.....
2
3
. 6
0.71
= 250.0 DEG. F
S02 CONCENTRATION
, ;.; : PPM
:''::'.: I'T.^:--" 2000'.'
1697.
1371.
1033.
2CoJoQr-fiiiSl
ACID LOADING
LBS ACID/LB CARBON
0. 1837
0.1527
0.1193
0.0846
:;,::;,-::s,;;::--.:-,:: ,,.,..: 0.0503.
?f:p^d^::;--. .-o.oias:
Wfiti&t&ti'-L 0..0
YOTAL":CARBON""REC!U"IRED = ; ;60".37
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 6.71
SPACE VELOCITY = 1984. 1/HR
PRESSURE DROP ACROSS CARBON _= ^P.-1? INCHES H20
PRE SSURE DRCP' "ACROSS"~PL ATES" -' "" "f5 .09""lNCHES""H2'd ""
TOTAL PRESSURE- DROP ACROSS STAGES = 45.27 INCHES H20
221
-------
S02 SORBER DESIGN
RUN NUMBER
TEST-24 DATE 7 27 71
TCTAL CARBON RATE = 45.470 LBS/HR _
"OUTLET CARBON LOADI "NG~~ = O.T8375 TBS ATTD7LO~T7iRBON'
HEIGHT OF CARBON/STAGE = 9.00 INCHES
DIAMETER OF VESSEL_= i?_._0__INCHES__ |
"CARBON USED~=~~ o.
TOTAL GAS FLOW RATE = 17033. SCFH
INLET S02 CONCENTRATION ^_ __ 200°'_ ?P1
INLET NO CONCENTRATION - " " i'50T "PP"M~
INLET 02 VOLUME FRACTION = 0.0460 :
INLET H20 VOLUME FRACTICN_= 0.1300 -:
"OUTLET""S02"CCNCENTRAT ION =
__
^OO.'P'PM"
TEMPERATURE = 275.0 DGG. F
S02
STAGE :
PPM
"AC rO"'LO'AD"lNG' .......
L8S ACIO/LB CARBON
1 .. -:-
3
4
*>
6
: 7
8
0.10
',. 2000.
1758.
1500.
1231.
957, :
688 . ;. j:>
220.
200.0001
'. " V s : o.i837
0.1589
0.1325
0. 1049
₯,:v.-:-../.-: .-.-vxaV; .;,-:'..:-., 0.0769
;.:gi:x:|-: x;:.; ^-:^.ff:yr, ?:?T: ; : : . Q . 0 4 9 4
f E^Miilll^ll^lC: 0.0236
0.0014
0.0
TOTAL CARBON REOU IRED_ =___ 7 2_._9 4 ^I_NCH E S ____ ___ _
"TOTAL STAGES REQUIREl)~ASSUMfNG 9.00 INCHES CAR~BW/ STAGE
____
= 8.10"
SPACE VELOCITY =
1586. 1/HR
PRESSURE DROP ACROSS CARBON =;;
PRESSURE DROP ^CRO'SS|]-AT_§S__=_
"
36.47: INCHES H20
18.23 INCHES H20
TOTAL PRESSURE DROP ACROSS STAGES =
54.70 INCHES H2O
222
-------
S02 SORBDR DESIGN
RUN NUMBER TEST-25 DATE 7 27 71
TOTAL CARBON RATE = *1.*980_ LBS/HR
OUTLET CARBON LOADTNG~= "O'Tl"8375~H'S"~AC1 WLTfTTRBOW
HhlGHT CF CARBON/STAGE = 9.00 INCHES
DIAMETER OF V E S S EJL_ =_ 18 . 0 _INCHIES_^
"CARHON"USEDi ="" ~ o."~ * ' ~"
TCTAL GAS FLOW RATE = 16473. SCFH
INLET S02 CONCENTRATION = _j?000_. PPM _
INLFT NO "CONCbNTRAT ION""= '" " " l50V "PPM':'~
INLET 02 VOLUME FRACTION = 0.0460 .;'"
INLET 1120 VOLUME FRACTION =__0_.J3qO _ ::;^
OUlLliT S02 CONC'ENTRAtTON""^" " ' "2'66. ~P"P~M"
TtMPERATURE = 300.0 DEG. F
' ~s"o
STAGE . .
2
3
8
9
0.72
;ONCENTRAf I'ON~" ""
PPM
: ;.; .2000.
1803.
1596.
1380.
115«,
0-3 C
^ ^ ^ *
716.
508.
319.
200.0C01
ACID LOAD ING" ~" ~"
L8S ACJO/L8 CARBON :
' .0.1837 ./%: :.'.
0.1636
0.1423
0.1202
0.0975
0 07^7
0.0522
0.0309
0.0115
0.0
TOTAL 'CARBON'Rif"QUTREU~= 87.44 INCHES"
TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 9.72
SPACE VELOCITY =.;,;,. ' 1279. 1/HR; \;-,,:..:f.'-M;,.,::;,:V: : ;.,.^?i> :,:;.>.-
PRESSURE DROP ACROSS CARCCN =' 43.72 INCHES H2Q1 ;___:
"PRESSURE" DROP"' ACRCSS^P'LATES' = " 21.86 INCHES H2b"
TOTAL PRESSURE DROP ACROSS STAGES = 65.58 INCHES H20
223
-------
APPENDIX A-10
REACTION RATE STUDIES FOR SULFUR GENERATION
IN 1 INCH DIAMETER FIXED BED
224
-------
RATE OF SULFU" GENERATION
BENCH SCALE
3 10 71
CO
Ul
- SG-72
SPACE VELOCITY
~ I'-E^T GAS CLCV.'
' *F:G"T CF
O.IOO'S^E Ofc /HI
T£ = 233.00 SCC/MlN
UNLCAC.-FD * 11.900 G-«S
LOADED
15.00 CMS
- INLET orBCE"jT u2s , 30.000
INLET "OLAR M2S CONCENTRATION
INLET SJLFURIC ACI2 LOADING
0.42B571 MOLES H2S/MOLE INERT GAS
0.206000 GYS H2S04/GM CARBON.
FINAL OJTL£T PERCENT SULFUR LOADING CN CARBON - is,040
FINAL C'JTL"* SULFUR LOADING ON CARBOA » 0.227 CMS S/GM CARSON
~ INITIAL TF.-'PERAT',-°E = 2"'C.CO F
wtxr-'jn' TEVOERATUPE « 355.00 F
FINAL TE^ERA-LRF - 302.00 F
TP'E
0.0
2.0
4.0
7.0
- 10.0
12.0
Ifc.C
16.0
- 15.0
20.2
- 22.0
24.0
26.2
2?.C
. 3C.O
32.0
- .34.0
36.0
3S.O
42. C
42.0
44,0
- 46.0
4P.O
52.0
~ 57.2
; 54.2
f ~ 0
- 5E.C
6C.O
62.0
T 64.2
6S.2-
PERCENT H2S
0.
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24023CE
2-4r02E
2 5-62 CO"
264000E
272003E
2 74002E
27320CF
2 7 « 2 T 2 E
27=OC2E
'27-r-2;F
, 2 i - Z ~ C E
i272202F
i 2 5 6 2 0 T E
2.256700F
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~.
LOA:
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ING «
00
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21
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PERCENT 502
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0. OOOCOOE
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0. OOOOOOE
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PERCENT coz MOLAR CONC HZS
0.
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.683760E-01
.82251CE-01
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190345E 02 --UNUTES
M2504 LOADING
J3MS ACID/OK C
0.206000E 00
' 0.1S1530E CO
0.157061E CO
0.121500E 00
o.eea&boE-oi
C.6369eS£-Cl
0.507661E-01
0.3&5569E-2i
C.25352CE-C1
C.l6lfc!)6E-Ol
O.B66C67E-02
C.202475E-C2
-C.A21576E-02
-C.964649E-02
-0.14Q561E-C1
-C.1772b8E-Cl
0.23561.-5C-C1
0.2626b6E-Oi
0.269716E-01
0.315? JOE-Oi
0.34E115E-01
0.381C.J4E-01
0.422512E-C1
-C.470749E-C1
50
-0.656274E-;!
-C.687628E-Oi
-C.7i6c49E-01
-0.7460S9E-C1
-0.775269E-01
-0.804479E-C1
-0.8775C5E-0'.
RATE ACIU
GX ACID/OM C-.XI.\.
O.OOOCOCt 00
-C.102»26:.-01
-0.9S865'-i-o2
-0.804'-l;>c-02
-C.613-'o»t-02
-0.509/74C-02
-0.408o6o--C2
0.34- s2»c.-02
-0.302i:3tit-02
-0.24118^t-02
-0.19947 ^t-02
-0.167;9/;-02
-0.14605it-22
-0.124266C-02
-0.16 /U9/L-02
-0.16 I'j'S ^L-C2
0.24iigjc.-02
-0.241. feiL-02
-0. 167^9 'L-02
-0.16 /V9/S-02
-0.16 '^9/c-02
-0.l46C5i£-02
0. 146C5.C-C2
-O.l46c5i--02
-C.l46o5.t-C2
-C.lfc6C-5iC.-OZ
-0.i46C5.i-02
;rF C- "Cli OECO'-'^OSiTION = -0.457S76E-02 AT 0.19C345E 02 MINUTES
vra*/;E =iTF OF ACID 0£CC"PCS IT I0\ UP TO ?C PERCENT ACID UTILIZATION
-0.931299E-02
-------
RATE OF SULFUK GENEKATION
BENCH SCALE
SG-?5
SPACF VELOCITY = 0.116^37E 04 /HR
INEPT GAS FLOW RATE * 5SJO.OO SCC/"*IN
WEIGHT OF CARBONt UNLOADED = 25.600 QMS
LOADED
32.20 CMS
INLET PERCENT H2S * 30.000
INLET MOLAR Has CONCENTRATION =
INLET SULFURIC ACID LOADING =
0.428571 VOLES H2S/MOLE INERT GAS
0.206000 GMS H2S04/GM CARBONt
FINAL OUTLET PERCENT S'JLFUR LOADING ON CARBON B 15.600
FINAL OUTLET SUL^U* LOADING ON CARBC\ » 0.196 GMS S/GM CARBON
INITIAL TEMPF9ATU9E » '270.00 F
MAXIMUM TFMPERATURF « 338.00 F
FINAL TEMPERATURE = 318.oo F
3 16 71
PERCENT H2S
PERCENT 502
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
O.OOOOOOE
O.OOOOOOE
O.OOOOOOF
0.240000F
0.7600COF
0.148000F
0.20600CE
0.266000E
0.296000F
0.300000E
00
00
00
01
01
02
02
02 -'
02
02
O.OOOOOOE
O.OOOOOOE
O.OOCOOOE
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-- - C. OOOOOOE
O.COOOOOE
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00
00
00
00
00
00
00
00
00
00
PERCENT C02
O.OOOOOOE 00
O.OOOOOOE 00-
0.OOOOOOE 00
O.OOOOOOE 00
0.0000'JOE 'JO
O.OOOOOOE 00
O.OOOOi-'OE 00
OiOOOOUOE -JO
O.OOOOOOE 00
O.OOOOOOE 00
MOLAR CONC H2S
H2S04 LOADING
GMS ACI-/GM C
RATE
O.OOOOCOE 00
O.OOOOCOE 00
O.OOOOOOE 00
0.245901E-01
O.S22510E-01
0.173708E 00
0.259445E 00
0.362397E 00
0.420454E 00
0.428571E CO
0.2060JOE 00
0.1776&6E 00
0.1493/2E 00
0.1218 l£-01
0.7722 '3E-01
0.6322iSE-Ol
0.5544V2E-01
0.5299»2E-Ol
0.527270E-01
O.OOOCO-- 00
»0«14i V6'^-01
-0. 14A ij6--<^-01
-0« 13i-!'41-'--01
-0«114-9?^-01
-C.84ictt^'--02
~0.55i:=-6-"--02
-0.21c-j9w^-02
-0«268i2*'t-c3
0.00^-Ovw 00
A+t* «f
0.773 f-
-------
RATE OF SULFUR GENERATION
BENCH SCALE
SG-2*
SPACE VELOCITY « 0.992250E 03 /HR
INERT GAS FLOW RATE « 309.00 SCC/MIN
WEIGHT OF CARBON* UNLOADED * 16.000 CMS
LOADED
20*00 CMS
INLET PERCENT H2S * 30.000
INLET MOLAR H2S CONCENTRATION »
INLET SULFUR 1C ACID LOADING *
0*428571 MOLES H2S/MOLE INERT GAS
0.206000 CMS H2S04/GM CARBONt
FINAL OUTLET PERCENT SULFUR LOADING ON CARBON » 18.400
FINAL OUTLET SULFUR LOADING ON CARBON * 0.229 GMS S/GM CARBON
INITIAL TEMPERATURE * 270.00 F ~ -
MAXIMUM TEMPERATURE - 321.00 F
FINAL TEMPERATURE » 303.00 F
3 11 71
ro
TIME PERCENT H2S
0.0 O.OOOOOOE 00
2.0 O.OOOOOOE 00
4.0 0.1600COE 01
6.0 0.440000E 01
8.0 0.820000E 01
10.0 0.114000E 02
12.0 0.154QOOE 02
14.0 0.186000E 02
16.0 0.196000E 02
19.0 0.2020COE 02
21.0 0.212000E 02
23.0 0.234000E 02
26.0 0.256000E 02
28.0 0.268000E 02
31.0 0.284000E 02
35.0 0.300000E 02
37.0 0.300000E 02
PERCENT S02
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOCOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
PERCENT C02
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
MOLAR CONC H2S
O.OOOOOOE 00
O.OOOOOOE 00
0.162601E-01
0.460251E-01
0.893246E-01
0.128668E 00
0.182033E 00
0.228501E 00
0.243781E 00
0.253132E 00
0.269035E 00
0.305483E 00
0.344086E 00
0.366120E 00
0.396643E 00
0.428571E 00
0.428571E 00
H2SC4 LOADING
GMS ACID/GM C
00
00
00
00
00
0.2C6000E
0.181864E
0.158187E
0.1358C6E
O.U5482E
0.974853E-01
0.820988E-01
0.695234E-01
0.586866E-01
0.434718E-01
0.34Q397E-01
0.260817E-Q1
0.173145E-01
0.131771E-01
0.919110E-02
0.739333E-02
0.739333E-02
ACID LOADING « 0.205999E-01 AT 0.248757E 02 MINUTES
RATE OF ACID DECOMPOSITION « -0.278624E-02 AT 0.2487S7E 02 MINUTES
AVERAGE RATE OF ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION » -0.709168E-02
RATE ACID DECOMP.
CM ACID/GM C-MIN.
O.OOOOOOE 00
-0.12067SE-01
-O.U6Q97t-Oi
-Q.844456E-02
-0.69419JE-Q2
-0.563J50E-02
C.449215t.-o2
0.34658 /t-32
0.237690E-02
C.175647E-02
O.OOOOOi-E OC
O.OOOOOOE 00
-------
RATE OF SULFUR GENERATION
BENCH SCALE
- SG-23
SPACF VELOCITY * C.100654E Oft /MR
- :*E»T GAS FLOW 9ATIT * 155.00 SCC/vlN
v.'FK'MT Cc CARBON. UNLOADED * 7.9»0 G«S
LOADED
10.00 CMS
INLET ocqcci,T _2s - 30.COO - - ---
INLET WOLAS H2S CONCENTRATION = 0.428571 «OLES H2S/MOLE INERT GAS
INLET SULPU"?IC ACID LOADING " 0.206000 GKS M2S04/GM CARBON.
PP.AL CUTLET = E = CE',. SULF'JS LOADING ON CARBON « 20.720
FI'.AL 0'JTL£T S'JL^L". LOADING ON CARBON « 0.260 CMS S/GM CARB3N
INITIAL TE"P£RAT'J'S » 270.00 F ' -----
MAXlvu* TE''3E'?ATU'fr = 330.CO F
FINAL TEvt>ERAT-j=£ 320.OC F
3 10 71
OO
TIVE
0.0
2.0
4.0
e.o
10.0 --
17.0
14.0
16.0
18.0
20.0 .
2?.0
24.0
26.0
2? . 0
3C.O
32.0
34,0 -
n f ft
Jc . 0
3f .0
40.0 "
44.0
46.0
-50. 0 -
53.0
56.0
'59.0
62.0
65.0
PERCENT H2S
O.OOOOOOE 00
O.tJOCOOE CO
0.1B4COOE 02
C.192000E 02
0.192COIE C2
0.1 92 CO
c.is-cc
C. 17400
0.15SCC
o.iseoo
C.:960U
c.2i-;:
C * 2 1 6 0 Z
*"" 2 1 ** " n
0.234::
0.214C3
C9 "a " ^ *
. / 1 -J - *
0.256"
0.2361C
0.23600
c.233:o
0.24-CC
0.25230
E 02
E 02
E S2
E 02
E 02
E C2
E C2
E 02
c f\2
E 02
E 02
E C2
r ^9
. u£
c 02
E C2
E 32
E C2
E C2
E 02
C.263C30F 02
C.270COCF C2
C.274rCDE 02
0.2">4COOE 02
PERCENT 502
O.OOOOOOE
- O.C30300E
O.OOOOOCE
0.000003E
0.030000E
O.OCOOOOE
O.OOOOCCE
O.OOCCOCE
O.OCC30CE
3.3C3C30E
c.occ3":oE
0.303C30E
C.303700E
f* r* ^, n ft ^i
S.SOO:OCE
O.C030COE
n o .-\ ,~\ A '\ c
C . u w ^ o u v ^
/> »>A«^/N^-^
'. u J ^ J J w'C
3. 003CC CE
C< 00><003E
O.OO;OOOE
O.OCCOOCE
- G.503033E
D.COCOOC'E
" O.OOOOOOE
OlOSS'OCc
:.300000£
00
00
00
00
CO
00
00
00
00
'.'3
uO
00
CO
r>"
00
30
00
AH
uu
00
S3"
00
CO
CO
00
00
oo
cc
so
PERCENT C02 MOLAR CONC H2S
0.
'0.
0.
COOOOOE
OOOO'JCE-
COOOOOE
O.OOOOOOE
o.
0.
0.
o.
0.
0.
c.
0.
c.
0.
0.
c.
0.
.
0.
o.
0.
c.
o.
G.
3 .
0.
0.
0.
OOOOOOE'
OOOOOOE
3000C3E
COCC-JOE
OOCOOOE
COOOOOE
COC303E
030CUOE
OOCOOOE
C300COE
030CCOE
OOOO'JOE
030030E
,T"Jf> "* -'* AF
U JU \- v/C
OOOOwOE
OOCCiOE
OOCOCOE
OOOOi-OE
OOOOC'.OE
OOOOOOE
OCOOJCE
OOOOv-OE'
OOOOuOE
OOOOOOE
00
CO
00
00
oo
00
00
03
00
00
oo
00
00
CO " "
00
00
co
o *\
J U
00
co
00
CO
00
30
CO
00
00
00
3.000COOE
00
0.401606E-C2
0.225490E
0.237623E
0.237623E
0.237623E
0.225490E
C.210S53E
0.21951IE
0.231527E
0.243781E
C.2722-64E
C.278772E
0.278772E
0.256281E
0.272264E
0.27B772E
07Q fc 7 1 1 ~
*t?D 'WA^
0.344086E
0.308900E
0.33890CE
0.312335E
0.329787E
0.336b98E
0.351351E
0.369S63E
0.377410E
0.37741CE
00
00
CO
00
CO
CO
00
CO
03
00
00
CO
00
00
00 ~
nf>
UU
00
30
00
CO
CO
00
CO
00
00
oc
H2S04 LOADING
G"S ACIO/GX C
0.206000E 00
0.131716E CC
0.163854E OC
0.1414^4? 00
0.1305;>4E 00
0.1196B5E 00
0.1084/OE 00
0.964S75E-01
3.843343J-01
0.727762E-01
0.619063E-01
0.522COCE-31
0.434!, ,'SE-Ol
C .3496C3E 01
0.257529E-01
O.l64403£-C'i
0.77279CE-32 "
»n 5~5Tri.c-.ra
O titJc i L*»!l v .*
-0.632314E-C2
-0.121438E-01
-0.257662E-D1
-0.3Z4327E-C1
-0.44722sE-Oi
0 .52fi50oE 01
-0.6006"4E-C1
-0.65c:676E-Oi
-0<"355£3E-Ol
-C.74926SE-C1
RATE Ado ^tCOi'.J.
G.»; ACID/CM C-XJ,,.
O.CCO^OOt 00
" -0.12063^-01
-0.57S014L-C2
0.54-3'»7*t-c2
-0.54J47>L-02
-0.54347*^-02
-0.576vl«-i-02
-0. 62024411-02
-0.59'-02 = t-02
-3.56oo3it-02
-0.526» = -.t-02
-0.444t)8pt-02
-C.426J6it-C2
fi ii. 7 A *ftir"*O?
-o!490i7>£-02
-C.444c8it.-02
-0.426;6i--C2
-0.24U464L-02
" -O.J4C,uC'l--02
-0. J4060'£.-02
-3.333=3.^-32
-C.2oll6At-C2
-0.260>2»t-32
-0.219 '3at-02
-C.16709/i-02
-C.l4ibl;t-32
-3.l4iifclac-C2
ACID LOADING = C.205999E-01 'AT 0.311104E 02 MI.NUTES
PATE Oc «CID :ECOVCOSIT!ON » -C.465116E-02 AT 0.31110'E 02 MINUTES
AVE°AGE ^ATE Cc ACJ3 Drr:'-'POSIT lOV U° TO 90 PERCcNT"ACIO UTIT.IZA" ION =
-0.571293E-02
-------
RATE OF SULFUR GENERATION
- BENCH SCALE
SS-?1
SPACE VELOCITY » 0.10<,59BE C
K>
VQ
Tf-'E
0.0
?.o
''.0
6.0
P. 5
11.0
13.0
15.0
1 7 . 0 - - -
19.0
21.0
22.0
25.0
?7.C
29.0
31.0
33.0
35.3
37.3
30. c
^ 1 C
**"'*«
51.3
5"". 3
c c . ^
61.0
O.OOOOOOE
0.1<>OOCOC
0.19<.COCF
C.2C630CE
C.2130Cr.F
0. 2?**CCOE
C.216000E
0.2C2300F
0.19»COO?
0.2C2033F.
C'.2?7330F
0.223333F
C.23S003E
0,2'T-030E
0.2'.B303E
C.2'-53C';E
3.25'-f)0'JE
0.203003E
C.2620COF
3.2h?OJ'-F
3.262"00C
c!2700^F
?:2~o3lE
C.2?6000F
C.290000F
C.2^^000r
0 . 3 ? 0 0 C ' E
OC
02
02
02
02
02
C2
02
02
02
C2
02
02
C2
02
C2
02
02
02
02
02
32
02
02
n *
vV
C2
32
0?
02
PERCENT 502
0.
0.
0.
0.
c.
0.
0.
0.
OOOOOOE
OOOOOOE
OCOOOOE
COOOO'JE
OOOOOOE
3033COE
C33300E
OOOOOOE
o.ooaoooE
c.
0.
0.
c.
0.
0.
c.
0.
0.
0.
0.
0.
Oi
3.
0.
0.
0
o.
0.
2,
1^
c.
0.
3333 3CC
3C303CE
C00003E
3 C C 3 3 C E
OOOOOOE
OOOOCOE
03303CE
OCOO~OE
03330CF
00333 OE
030000F
30300CF
^ f\ A f> ^ f* jT
OOVOCCE
05000 OH
OCU33CE
00303CE
scjoccE
ccom-E
OOOOOOE
0003C!'E
3C333CE
OC03"'.'E
00
00
30
00
00
00
00
03
00
CO
00
CO
30
03
30
03
00
00
oc
CO
03
00
30
03
00
OC
03
00
30
00
00
CO
0
0
o
0
ft
. . Q
0
0
c
0
0
c
0
0
C
c
PERCENT C02 MOLAR CONC M2S
.OOOOOOE
.OOOOOOE
.OOOOOOE
.0030UOE
. OOCOoOE
. OOOOOOE
.OOOOJOE
.OOOO'-JOE
.OOOOUOE
. OOOO'JOE
.0000-CE
. OOOO'JOE
.0030JCE
.0300UQE
.OOOOCOE
.0000 JOE
C.COOO~OE
0
0
0
c
c
r<
' 0
0
0
._ £
0
Q
0
0
c
.ooaoooE
.OC30JOE
,C300,;OE
.0000 OOE
.COOOJOE
.CCOOJOE
.OOOOJOE
OOOOJOE
.U030UOE
30UOJOE
. OOOO'JOE
.OOOO'TOE
.3COCJCE
.OOOOJOE
.O'iCOi'OE
00
oo
oo - -
oo
i>0
,ao
JO
00
yQ
JO
JO
30
JO
JO
30
UO
JO
00"
JO
JO
'00
DO
'JO
00
00
JO
oo
30
00
CO
JO
1/0
O.OOOOOOE
0.162790E
0«2'>069'tE
0.259i't5E
0.265822E
0.288659E
0.275510E
0.253132E
0.2'-6BB2E
0.253132E
0.2B2051E
0.295336E
0.3C3903E
0.322751E
0.329787E
0.329787E
0.3<.C''82E
0.3'.770SE
0.355313E
0.355C13E
0.355013E
C.369863E
C.369663E
0.377410E
0.377410E
0.3950'tlE
0.392757E
0.403560E
O.^OE'-SOE
0.^16A33E
3.^28571£
O.'.?f 571E
00
00
00
oo
00
00
00
00
00
03
00
00
00
00
00
00
00
00
00
00
00
CO
03
00
00
00
03
oc
00
cc
CO
00
M2S04 LOADING
GMS ACI3/GM C
0.2063JOE 00
0.165L-02
-0.1511'3'.t.-o2
wGwE. 00
JO.- oo
:3 LO'Di-.r, = 3.205990^-31 />r c.<-662ieE 32 «INUTES
E C= ;C1D SECCVDOS: r!0\ = -0.155761E-02 AT 0.<»66218E 02 MINUTES
E'AJE si'r OF ACIC OrCO-'''»OSlTiO>: u-> TO 90 PERCENT ACID UTILIZATION «
-0.373*63E-C2
-------
KATE OF SULFUR GENERATION
BtNCH SCALE
1 71
SG-<»3
SPACt VELCClf'Y = " "b". 309191E 03 /HR
INERT GAS FLOW RATE = 7064.00 SCC/MIN
WEIGHT UF CARBONi UNLOADED = 1179.000 GMS
LOADED
1486.00 GHS
INLET PERCENT H2S = 29.700
INL§T_MOL_AR H2S CONCENTRATION = 0.422475 MOLES H2S/MQLE INERT GAS
INLET suLfURIC ACIO LOADING""« o.i366oo GMS H2S04/GM~CARBUN,
5.INAL OUTLET PF.RCENT SULFUR LOADING ON CARBON = 21.080
"FINAL OUTLET SULFU«" LOADING ON CARBON = " 0.266 GMS S/GM CARBON
INITIAL TEMPEKATURE = 290.00 F
MAXIMUM TEMPERATURE = 3*0j-?ll_f
FINAL TEMPERATURE = ""320^00 > . " ~ ~~
to
U>
o
TIME
0.0
10.0
20.0
30.0
40.0
50.0
60.0
70. 0
60.0
90.0
100.0
110.0
ACID
RATE
PERCENT H2S
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.270000E 02
0.290000E 02
0.29^0006 02
0.297000E 02
0.280000E 02
PERCENT S02 PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
LOADING = 0.136000E-01 AT
OF ACID DECOMPOSITION = -0.
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.331655E 02 MINUTES
3690596-02 AT 0.331655E
MOLAR CONC H2S
0.0
0..0
0.0
0.0
0.0
0.0
0.0
0.369863E 00
0.40B451E 00
0.
-------
RATE OF SULFUR GENERATION
BENCH SCALE
SG-44
"SPACE VELOCITY = 0.309191E 03 /HR~
INERT GAS FLOW RATE = 7064.00 SCC/KIN
WEIGHT OF CARBON, UNLOADED = 1179.000 CMS
LOADED
1486.00 CMS
INLET PERCENT H2S = 29.000
INLET MOLAR H2S CONCENTRAT ION_ =
INLET SULFURIC ACIO LOADING =
__ 0.408451 MOLES H2S/MOLE _
"0.136000 CMS H2S04/GM CARBON,
GAS
9 2 71
FINAL OUTLET PERCENT SULFUR LOADING ON CARBON
FINAL OUTLET SULFUR LOADING"ON CARBON =
INITIAL TEMPERATURE = 250.00 F
_MAXIMUM TEMPERATURE = 355.00 JF
FINAL TEMPERATURE ="" " 310".00 F "
22.040
0.278 GMS S/GM CARBON
THE " PERCENf H2S
to
u>
0.0 " 0.0
10.0 0.150000E 01
_20.0 0.130000E_01
30~.0 6.930000E" 01 "
40.0 O.ll^>000t 02
50.0 0.145000E 02
""60.0 0.270000E 02
70.0 0.285COOE 02
80.0 0.290000E 02
"90.0 " 0.293000E 02~
100.0 0.290000E 02
110.0 0.29COOOE 02
PERCENT 502
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
OOOE-01 AT 0.387428E
ION = -0.246304E-02 AT
PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
o.o :-'
0.0
0.0
0.0
0.0
02 MINUTES
0.387428E
MOLAR CONC H2S
0.0
0.152284E-01
OM31712E-01
0.102536E 00
0.129943E 00
0.169591E 00
0.369863E 00
0.398601E 00
0.408451E 00
0.414427E 00
0.408451E 00
0.408451E 00
02 MINUTES
H2
GM
^i
»
i
-l
-l
-i
i
H2S04 LOADING
GMS ACID/GM C
~ACI"D OECOMP".
GM ACID/GM C-KIN.
0.100984E 00
0.665441E-01
0.359172E"-01
0.103907E-01
-0.122069E-01
-6.243253E-Or
-0.264410E-01
1°-JL26 871 2E- 0 1_
-0.266lOiE-01
-0.263491E-01
-0.263491E-01
0.0
-0.343504E-02
-0.345301E-02
-0.2672366-02"
-0.243294E-02
-0.208659E-02
ACID LOADING = 0.:
RATE OF ACIO DECOKPO!
"AVERAGE RATE OF ACID DECOKPO'SITION UP TO 96 PERCENf ACID UTILIZATION = -o.302348E-02
0.860399E-04
0.0
6.52205~9E-64~
0.0
0.0
-------
OJ
RATE OF SULFUR GENERATION
BENCH SCALE
9 2 71
SG-45
SPACE VELOCITY = 0.528427E 03~~/H~S
INERT GAS FLOW RATE = 11827.00 SCC/MIN
JUL!GHT_PF" CARbO.M, UNLOADED = 1151 ..Oqo. QMS
LOADED
1451.00 CMS
INLET PERCENT H2S = 30.000
INLE_L_MOLAR JH2S CONCENTRATION^ 0.428571 MOL|S_M2S/MCIL£ INERJ GAS
INLET SULFUR 1C ACID' LOAD ING" = O."l3600~0 GMS~ H2S04/GM CARBON",
JF INAL_ OUTLET _f>ERCENT SULFUR LOADING DN CARBON «
FINAL OUTLET SULFUK LOADING ON CAiRBON =
INITIAL TEMPERATURE = 260.00 F
_MAXIMUM TEHPERATURE_=_ 315.00_F
FINAL TEMPEKATURE = 300.0b"F
20.400
0.257 GMS S/GM CARBON
TIME
" b.o
10.0
20.0
30.0
40.0
50.0
ACID
*ATE
PERCENT H2S
0.0
0.100000E 01
0.185000E 02
0.270000E 02
0.300000E 02
0.300000E 02
PERCENT S02
0 = 0
0.0
0.0
0.0
0.0
0.0
LOADING = 0.136000E-01 AT 0.2641306
CF ACID DECOMPOSITION = -0.164731 E-02 AT
PERCENT CC2
0.0
o.o .' ;:,. ,
0.0 - "- -.
0.0
0.0
0.0
02 MINUTES
0.264130E
MOLAR CONC H2S
0.0
0.101010E-01
0.226994E 00
0.369863E 00
0.428571E 00
0.428571E 00
02 MINUTES
H2S04 LOADING
GMS ACID/GM C
0.136000E 00
0.725501E-01
0.261037E-01
0.660623E-02
0.220852E-02
0.220852E-02
RATE ACID OECOMP.
GM ACID/GM C-MIN.
0.0
-0.626933E-02
-0.301994E-02
-0.879543E-03
0.0
0.0
AVERAGE RATE OF^ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION
-0.391689E-02
-------
RATE OF SULFUR GENERATION
BENCH SCALE
SG-46
SPACE VELOCITY'S o.930io7E 02 YHR ""
INERT GAS FLOW RATE = 2392.00 SCC/MIN
HEIGHT OF CARBON, UNLOADED = 1124.000 CMS
LOADED
1417.00 CMS
INLET PERCENT H2S = 18.000
JNLET MOLAR H2S CONCENTRATION =_
INLET SULFURIC ACID lOADING" ="
_ °-2A9!1.2 MOLES H2S/MOLE JNERT_GAS_
0.136000 GMS H2S04/GM CARBON,
FJNAL OUTLET PERCENT SULFUR k°ADI_NG_ ON CAR30N
FINAL'OUTLET SULFUR LOADI.NG'ON CARBON =
INITIAL TEMPERATURE = 255.00 F
MAXIMUM TEMPERATURE = 3
-------
RATE OF SULFUR GENERATION
BtNCH SCALE
1 71
SG-47
SPACE VELOCITY = 0.7749276 03 /HR
INERT GAS FLOW RATE = 16584.00 SCC/MIN
_*l£iGHl_UF CAR3QNt_UNLpADEi}_5 1126.000 CMS
LOAD£0
1419.00 'CMS
INLET PERCENT H2S = 27.300
INLET HULAR H2S CONCENTRATION =
INLET SULFURIC ACID LOADING =
0.375516 HOLES H2S/HQLE INERT GAS
0.136000 &MS H2SO4/GM CARBON.
JLINAL__OUTLET_ PERCENT SULFUR LOADING ON CARBON
FINAL OUTLET "SULFUR LOADING ON CARBON =
INITIAL TEMPERATURE = 250.00 f
_MAXIMUM JLEMPERATURE_^ 385.00 F
FINAL TEMPERATURE = 310.00 F
20.44Q
0.258 GMS S/GM CARBON
U>
TIME
0.0
10.0
_ 20.0
30.0
40.0
50.0
PERCENT H2S
0
0
0
0
0
0
.0
. 182000E
.Z27000E
.260000E
.266000E
.273COOE
02
02
02
02
02 _.
PERCENT S02
0
0
0
0
0
0
.0 ,
. 0
.0 . . ...:.;,-. .
.0
.0
.0
PERCENT C02
0
0
0
0
0
0
.0 ;
.0 :£-. ..::-:;
.0 , ,.-;^"-. ::"'
.0
.0
.0
MOLAR CONG H2S
0.0
0.222494E
0.293661E
0.351351E
0.362398E
0^3755166
00
00
00
00
00
H2S04 LOADING RATE ACIt) iJECOKP.
GMS ACID/GM,C GM ACID/GC C-KIN.
0.136000E 00
0.792515E-01 ';
i0.54.0331E-01
0.426499E-01
0.386470E-01
0.372385E-C1
0.0
-0.328595E-02
-0.175773E-02
-0.518fc98E-03
-0.281692E-03
0.0
-------
RATE OF SULFDK GENERATION
BENCH SCALE
9 2 71
SG-48
U>
SPACE VELOCITY = 0.101530E 04 /HR
INERT GAS FLOW RATE = 22383.00 SCC/KIN
.EIGHT OF CARBON, UNLOADED * 1134.000 CMS
LOADED -
1429.00 GMS
INLET PERCENT H2S = 33.800
INLET'MOLAR H2S CONCENTRATION f
INLET "SULFURIC AC 10 LOADING ~="
_ 0.510574 HOLES H2S/MOLE INERT GAS
0.136000 GMS H2S04/GM CARBON,"
FINAL OUTLET PERCENTJSULFUR LOADING ON CARBON =
FINAL OUTLET SULFUR LOADING"ON CARbON =
INITIAL TEMPERATURE = 250.00 F
MAXIMUM TEMPERATURE, f 385.00_F
FINAL TEMPERATURE = ~ 290.~00 F
19.080
0.240 GMS S/GM CARSON
TIME
0.0
10.0
PERCENT H2S
0.0
0.219000E 02
0.324000E 02
PERCENT
0.0
0.0
0.0
0.338000E 02 0.0
IING = 0.1360COE-01 AT
S02 PERCENT C02
0.0 V
0.0
0.0
0.0
0.142038E 02 MINUTES
MOLAR CONC H2S
0.0
0.280410E 00
0.479290E 00
O.510574E 00
H2S04 LOADING RATE
GMS ACID/GM C GM I
0.136000E 00
0.294148E-01 ' -
-0.820515E-02 ' -
-0. 127066E-01
RATE AC'ID DECOMP.
GM ACID/GM C-MIN.
30.0
RATE OF ACID DECOMPOSITION = -0.421767E-02 AT 0.142036E 02 MINUTES
AVERAGE RATE OF ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION = -0.591159E-02
0.0
-0.662369E-02
-0.900292E-03
0.6
-------
RATE OF SULFUR GENERATION
BENCH SCALE
9 2 71
SG-49
SPACE VELOCITY = 0.181932E 03 /HR
INERT GAS FLOW RATE = 2*32.00 SCC/MIN
WEIGHT OF CARBQNt UNLOADED = 1118.000 CMS
LOADED
1409.00 GKS
INLET PERCENT H2S = 57.000
INLET MOLAR H2S CONCENTRAJION_*_
"INLET SULF-URIC ACID LOADING =
1.325531 MOLES H2S/HOLE INERT GAS
0.136000 GMS H2SOWGH CAROON,
_fJNAL_OUTLeT _PE_RCENT SULFUR. LOADING ON CARBON
FINAL OUTLET SULFUR LOADING ON CARBON =
INITIAL TEMPERATURE = 250.00 F
MAXIMUM TEMPERATURE 5 385.00 J:
FINAL TEMPERATURE = 275.00 F
16.360
0.206 GMS S/GM CARBON
U>
TIME
0.0
10.0
_2p.«P_
30.0
38.0
AVERAG!
PERCENT H2S PERCENT S02
0.0 '-'-' 0.0
0.0 0.0
0.220000E 02 0.0 .
0.325000E 02 0.0
0.<»50000E 02 0.0
PERCENT C02
0.0
0.0 :
o.o ;'...-. .';
0.0
0.0
MOLAR CONC H2S
0.0
0.0
0.262051E 00
0.481481E 00
0.818182E 00
H2S04 LOADING
GMS ACID.'GM C
0.136000E 00
0.939578E-01
0.56388^E-01
0« 26
-------
RATE OF SULFUR GENERATION
HtNCH SCALt
2 71
SG-51
SPACE VELOCITY = 0.105J47E 03 /HR
INFRF r,AS FLOW KATE = 2446.00 SCC/MIN
ViblGHT OF tARBONt UNLOADED = 1194.000 GMS
LOADfcO
_L505. 00 _GMS
INLET PERCENT H2S - 34.500
JNLET MOLAR H2S CONCENTRATION =
INLET SULF4JRIC ACID LOADING =
0.526718 MOLES H2S/MOLE INERT GAS
0.136000 GMS H2S04/GM CARBONf
_FJNAL_pUTLET PERCENT SULFUR LOADING ON CARBON = 13^840
FINAL OUTLE'T"SULFUR" LOADING ON CAR"BON =
INITIAL TEMPERATURE = 235.00 f
"F INAL TEMPERATURE"~» 2io.Fo "F" ~ ~~
0.174 GMS S/GM CARBON
LO
TIME
0.0
10.0
20.0
30.0
40.0
50.0
60.0
: 70.0
80.0
90.0
100.0
110. 0
120.0
130.0
140.0
~"ibo.o
160.0
170.0
IBO.O
190.0
200.0
210.0
PERCENT H2S
0.0
0.0
0.0
OvO
0*0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.540000E 01
0.188000E 02
0.235000E 02
0.360000E 02
0.310000E 02
0.345000E 02
0.345000E 02
0.345000E 02
PERCENT S02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0 __
0.0
0.0
0.0
0.0
0.0
0.0
0.0
PER(
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
ENT C02 MOLAR CONC H2S
0.0
. ::--;,:'-.. ;- 0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.570825E-01
0.231527E 00
0.307190E 00
0.562500E 00
0.449275E 00
0.526718E 00
0.526718E 00
0.526718E 00
INUTES
H2S04 LOADING
GMS ACIU/GM C
0.136000E 00
0.120268E 00
0.104536E 00
0.888035E-01
0.730713E-01
0.573392E-01
0.416071E-01
0.256749E-01
0.101428E-01
-0.558928E-02
-0.213214E-01
-0. 370535E-01
-0.527856E-01
-0.685177E-01
-0.833973E-01
-0.948193E-01
-0.1025C6E 00
-0.105250E 00
-0.105872E 00
-0.1G7029E 00
-0. 107029E 00
-6.107029E 00
RATE ACID OECOMP
GM ACID/GM C-MIN
0.0
-0.157J21E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.140272E-02
-0.881682E-03
-0.655691E-03
0. 106P76E-03
-0.231306E-03
0.0
0.0
" 0.0 "
ACID LOADING = 0.136000E-01 AT 0.77802'>E 0;
RATE OF ACID DECOMPOSITION - " -0. 1573^2IE-02 AT 0.778025E 02 MIMUTES
AVERAGE RATE OF ACID UECtHPOS1TIUN UP TO 90 PERCENT ACID UTILIZATION * -0.157321E-02
-------
APPENDIX A-11
SULFUR GENERATION EXPERIMENTAL DATA
238
-------
-'OS-.! SuLJTJr. AMD SC-2 AZ^IYSES 01C CAKBGN
AS A FU:::YI.;IC D? IBS ?cs nux DSC-?
/ " O ~~ a TI > . . - . -H - _ _ _ \
Vc2> F fc.t >o".; -^S ar.^. 0 -j r.C;
IOTA.L SUIFuK AHD S02 AKA.LYSES ON CARBON
AS A FUuCIIOS OF SIK3 FOR Hull 3SG-8
( 325°? s.t 1C % H2S and 0 % H20)
i
i
Elapsed Ti.-e ,
=in. 'IOC
Total Sulfur, j SOg Analysis, * 1
^ ! Its. S02/100 TDS. C
C j 5-3 i 14.63
r - ' ' " -, -, i
C . ~ ' ; - i-
! ?'- ; ^-3 i 17.6
i;c
n 0 r
7-6
7.2
18.2
16.4
i 15-' 3.5 i 13-95
: 175 : C.4
^ r
235 9-6
to
U)
VO
260
230
~-'0
330
^--^
;.cu
390
425
450
1^90
1
9-1
9-7
9-4
1C. 4
11.8
10.5
11-5
12.21
11.18
9-4
8.56
7.5
6.4
5-52
^-75
4.1
3-56
3-12
2-95
* Meaz-orei SO; evolution oy H202 corubb:r.g when careen
heated LO 1000°F
Elapsed Tice,
tain. /ICO
0
20
1*0
60
30
100
120
iko "
160
180
200
220
21)0
260
280
300
320
3l+0
360
380
ItOC
420
1*40
1*60
1)80
500
Total Sulfur,
%
6.48
7.40
8.00
7-92
8.44
8.72
9.12
9-76
9.80
9-6
10.04
10.48
n.32
11.48
3J..68
11.96
12.4
12.60
13.08
11.6
13.4
13.3
13-68
13.4
13.96
14.52
S02 Analysis,
Ibs. SOp/100 Ibs. C
14.77
17-53
19-57
19-36
16.95
16.00
14.38
13-75
12.85
11.26
9-93
9-96
7.80
6.46
5-54
5-19
4.75
3-73
2.94
3-27
3-03
2.82
2.64
1.54
2.27
2.73
-------
Cr-l:-L S'Jui?. >.;._/ S02 AlilYSSS C"..' CA.KECii
AS A JLI;CIIO:; o? II:-E ?CR ?.~j~.\ rs^-9
15
0 ; X2C)
TOTAL SULFUR AKD S02 ANALYSES OK CARBON
AS A FUNCTION CF TE-E FOR ROT DSG-10
( 325 °F at 20.8$ HgS and 0 $ E2o)
to
4>
O
-in. /IOC
.
-
*"
1 ^
\ '-'
; 55
75
95
» -, c
I ^-*>
i i>5
1 175
200
220
260
520
550
275
4oo
425
450
475
500
Tccal Sulfur,
7 " -
I . v,'^
7.&0
S.32
8.08
9.c4
9.16
9-88
10.20
1C. -2
10.52
12.0
12.76
13-60
14.04
14.23
14.08
14.60
14.52
14.60
14.76
15.20
SCp Analysis,
Its. 30? ICO Its. C
** r^7
17.4
1S.T3
16.28
16.96
14.48
12-73
12.53
11.04
9-73
8.57
4.47
3-39
3.70
3-13
2.98
2.58
2.97
2.96
2.64
3-06
Elapsed. Tiae ,
min . /ICO
0
10
30
50
75
100
225
150
175
200
225
250
275
300
325
350
375
400
425
450
475
500
Total Sulfur,
*
6.0
7-7
8.5
8.7
9-8
9-6
io.4
11.4
11.5
12.5
13.5
13-7
14.3
15-3
14.0
15.4
14.1
14.9
15-2
15-4
14.6
14.8
302 Analysis
Ibs. S02/100 Ibs. C
15-1
18.3
19-6
17.5
13-9
11.5
9-26
9-14
8.02
6.64
5-23
3-97
3-58
2.70
2.76
2.35
2.S3
2.38
2.68
2.65
2.39
-------
T03VL SUJVFUR AM) 302 AIK.LYSSS CN CA.B30N
AS A ?-JI\CTIOH OF 3II/S FO?. EUII DSC-12
( 315°? at 5-3$ H2S and 30 %
Slapsed Tie, ! -CTs.1 Sulfur, ZC-.- Analysis
- '"0'^ ' ;'- ' "v>s. SCs'lCO loo. C
; t
>-r - r * - : -,
1 < , 1 - .- - *
ic ; E.S: i 18.76
*."'
! =z
i
11-1
O.lj
15.4
1C . 12 1- - 5
ic. :s
12.43 1
11. f-' 11-42
I ^ , 12. oO i 7-~~
t
150
175
N> 1 20C
+> 225
13-32
14.20
15.20
15.44
1-1 2?0 | 16. vO
6.69
5-36
3.92
2.86
2,50
275 I 15-50 2.765
325 16 . c
350
375
I }. -^f^
1 425
450
475
500
16.64
16.46
16.76
17.00
16.04
17.20
16.46
2.449
2.248
2.42
6.49
2.41
2.65
2.175
2.53
Elapsed Time,
min./lOC
0
15
22
to
70
100
125
150
200
250
275
300
Total Sulfur.
%
6.4
6.60
8.4
7.03
7-52
7-2
7-36
7-^
7-96
8.0
8.20
7-84
SOg Analysis
IDS. SC2/100 its. C
16.08
17.30
16.8
17.04
17.34
17.48
17-74
18.8
17.28
17.48
16.80
-------
TOTAL SULFIG. AID C02 Al^LYSES 01' CA.-iQ:
i 51:;F it 5-3f; H23 ar.d 20 ;', >;2c)
TOTAL SUEF^ A:E 302 AIALYSES oic CAI^D
AS A FUHCTICH 0? TBS FOR RUN DSC-i
5-3-5 H23 and 1C£ :-I2o)
£i;in!/icr'
cf
! :
' C j 6.6t
1C ! c.20
S02 Analysj.3
Its. SC2/1CO 1'os. C
15.5
17-1
JO ! 7 .2,6 : lD.92
50 i 7-20
! 75 ! 7-12
I ICC ! c.OO
17-73
17.6
17. 6t
I :^r : 7--o ! 17.25
; 150
"75
N3 2CO
-P-
N>
225
2C0
~-~"^
! ~~^
''. 350
too
't25
7 V" ' 17 £8
j . ~~r ^- 1 . '-'^
3. CO
7-2t
3.32
S.co
o.bO
17-99
17-73
17.93
17.9
15.68
? 0- ! -'5.68
8.12
8.20
6.8t
15- 3t
It. 32
It. 57
Elapsed Tims .
nin./100
0
25
ko
6c
75
100
125
150
175
200
225
250
275
300
325
350
375
too
1*25
t50
t75
500
Total Sulfur,
",j
( ^
7.00
7.2t
7.12
7.52
7-36
7-12
6.96
7.2t
8.0
7.2
9-28
8.60
6.8
8.60
9.00
8.92
7-6t
7-72
7.36
8.68
9-6
S02 Analysis
Its. SOa/100 Its. C
18.15
l'^92
16.63
15. t3
20.3
21.1
18.0
17-3
17.63
18.2
15.65
15.2
13-35
13. 7t
Ik.kd
12.76
10.83
10.6
9-96
9-26
9-39
8.t7
-------
TOTAL SULFUR AJSD SC>2 ANALYSES OS CAHBOH
AS A FUNCTION OF TIM3 FOR HUN DSG-15
TOTAL SULFUH AND SOg ANALYSES ON CARBON
AS A FUNCTION OF THE FOR RUN DSG-16
(275 °F at
E23 and 0 %
( 275°F at
and
U>
| Zlapsed Tine,
nin./lOO
I ,
0
15
30
50
75
100
125
15C
175
200
250
275
300
350
375
VOG
1*25
1*50
!*75
500
Total Sulfur,
/-'
6.12
e.kk
6.51
7.62
7.68
7.72
8.00
8.08
8.96
9-00
8.2
9.0
9.2
10.0
10.1
11.0
11.2
_11.2
, "l0.8
11.1
502 Analysis ,
los. SCto/'lCO Ibs. C
1
11*. 1
15-5
16.3
15-8
lit. 5
U.2
13.7
12.9
12.4
12.05
11.29
10.12
9.32
S.29
9.12
7-51
6.90
6.60
7-03
5-j 35
Elapsed Time,
min./lOO
15-
30
50
75
100
125
150
175
200
225
250
300
325
375
koo
1+25
450
U75
500
Total Siilfxir,
%
6.1
7. U
7.8
8.9
9.7
.10. ^
9-6
10.6
10.8
11.2
11.3
10.1
11. k
11.8
12.1
13.8
13.3
13.5
13.7
S02 Analysis,
Its. SQ2/100 Ibs. C
15; 80
15-19
13.75
12.21*
11.50
9.25
B,6k
7-73
7-^3
6.97
6.28
5-57
lj.75
U.W
^.99
3.1*3
U.31
3.37
-------
-CTA1 SULFy? A1C2 502 AlIAliSZS Oi: CA330K
AS A FuiiCTic:; :? :r~-z ?o?. ?:j.i 330-17
( 2?5°F at 25-4$ EgS and 0 % ;-;23)
TOIA.L SULFUR ACT S0£ AKALYSES ON CARBON
A3 A FUNCTION OF TBS FOR RUN DSG-18
! 325 °F at 5-0-p H2S and 0 % H20)
Slapsea Tine, I Total sulfur, ! 302 Analysis,
-in./ICO * ' Has. SCc/lOO Its. C
N)
0
20
40
s^ w
.
6. 84
15-23
9.6 10.99
9-1- ! 9-79
; 30 11.72 ! 7.5
j 125 i 11-25 6.47
150
175
225
250
275
3.00
325
350
375
400
425
450
475
500
12.60 5-68
13-52 4.36
14.12
13.76
13.54
5.6
4.38
4.86
15.0 : 4.9
14.48 3.74
15.0 ! 3-93
15.2
15-32
14.68
15-72
3.24
3.64
4.97
5.28
14.8 5-6
15.36 5-19
Elapsed Tine ,
min./iOC
0
20
40
60
30
100
125
150
175
225
250
275
300
325
350
375
i|00
1+25
450
475
500
Total Sulfur,
%
6.7
6.6
6.8
7-1
8.2
7-3
5.8
6.8
7-1
7.1
7.2
3.1
8.8
9.8
9A
___
""
S02 Analysis
Ibs. S02/1CO Ibs. C
15.1
15-7
16.44
16.0
15.0
14.5
13-1
12.0
8.75
8.45
8.62
6.57
5.6
4.95
4.66
4.32
4.06
3-7
4.36
3-93
-------
TOBi.Ii SULFUR AND S02 ANALYSES ON CARBON
AS A FUNCTION OF TIME FOR HUH DSC-19
( 325"F at 9-1% H2S and 0 % H2C)
TOTAL SULFUR AHD S02 ANALYSES OK CARBON
AS A FUNCTION OF TIMS FOR RUN DSG-80
( 325"? at 18.2$ EgS and 0 % H20)
N>
-P-
Elapsed Tine,
» - -V, / ~ f*f\
la^Ji . » .JLVW
0
j-5
30
50
Total Sulfur, |
ci i
8.5
6-9
S.O
7-9
75 " 8A
100 | 8.5
125
150
.L'f ^>
200
225
250
275
300
350
375
Uoo
^25
ir50
VT5
500
8.5
9-1
10.2
10.1
10,2
10.8
11.7
H-9
12.0
13-1
12.8
12.6
12.2
Z2..1
32.. 3
S02 Analysis
Ibs. S02/100 IDS. C
16.1
16.21
15-33
lit, 65
12.92
ll.C-7
9-25
7-96
7-52
6.22
if. 78
3-75
3.82
3^5
3-31
2.94
3-21
2.97
3-05
2.95
3-25
Elapsed Time,
min./lOO
0
15
35
65
100
125
150
175
200
250
275
300
325
350
375
425
if 50
VT5
500
_
Total Sulfur,
5-9
7.8
8.2
9.5
11.3
10-9
11-5
12.8
13-2
13.3
13. if
13.7
lif.5
13.5
13.3
13.lt
14. 5
13.2
14.5
S02 Analysis,
Its. S02/100 Its. C
15.0
l6.3
14.6
12.0
9-16
T.05
6.25
4.68
4.6
3-49
3.38
3.52
3.19
3.19
3.6l
4.03
3.48
2.99
4.13
-------
TOTAL SULFUR AJO) SO 2
( 325°? at 26.~: EC
^jYSi.5 s^_\ CAR30I7
?0a BUS DSC-21
=id C 5 K2C)
TOTAL SULFUH A3D S02 ANALYSES OH CARBON
AS A FUNCTION OF TIME FC3 RUN DSG-22
(325 °F at 37-6£ H2S and 0
to
ilapsed Tide,
ain . /ICO
;
0
25
50
t '
i '^
! 3?
100
125
150
175
200
225
250
275
300
i 325
i 350
j 375
too
! t25
t50
t75
500
Total Sulfur, '. £0g Analysis,
;1 1 Ibs. SOg/iOO Ibs. C
7.6
6.t
10. '*
11.3
12.3
12.6
15.5
T 5 £
13.9
it. 9
15-1
15-0
15.1
15-2
it. 7
15-2
15. c
15.0
15.3
15- 1
15 A
15.21
16.52
12.3
10.73 I
9-7
7-95
6.31
5.02
4.19
3.77
3.59
3.37
3.12
3.37
I'M
3.33
2.86
j 2.6
2.83
1.13
3-03 .
Elapsed ?ine,
min . /100
0
20
t5
70
100
125
150
175
200
225
250
300
325
350
375
too
1*25
450
t75
500
To-jal Sulfur, .' SOg Analysis,
% | Ibs. S02/100 Ibs. C
6.t
8.0
9.1
11.6
It. 3
It. 2
lt.0
It. 7
15.0
15.3
it. 7
15.lt
It. 7
It. 7
It. 3
16.2
15.5
13.7
It. 2
15.1
15.03
13.39
9.37
7.12
t.35
t.05
t.2t
3-30
3.39
2.85
2.33
2.5
2.76
3.35
2.29
2.61
3.53
5-38
2.76
2.81
-------
APPENDIX A-12
DETAILED RESULTS OF INTEGRAL RUNS
Page
1. Experimental Data and Results for Integral 248
Run IR-1-4 (188 - 243 hours)
2. Experimental Data and Results for Integral 260
Run IR-1-5 (246 - 262 hours)
3. Experimental Data and Results for Integral 271
Run IR-2-6 (37 - 51 hours)
4. Experimental Data and Results for Integral 283
Run IR-2-6 (51 - 66 hours)
5. Experimental Data and Results for Integral 295
Run IR-2-7 (66 - 81 hours)
6. Experimental Data and Results for Integral 307
Run IR-2-7 (81 - 96 hours)
7. Experimental Data and Results for Integral 319
Run IR-2-7 (96 - 111 hours)
8. Experimental Data and Results for Integral 331
Run IR-2-7 (111 - .126 hours)
9. Experimental Data and Results for Integral 343
Run IR-2-8 (144 - 148 hours)
10. Experimental Data and Results for Integral 354
Run IR-2-8 (148 - 156 hours)
i
i
11. Experimental Data and Results for Integral 365
Run IR-2-8 (156 - 168 hours)
247
-------
APPENDIX A-12-1
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-1-4 (188 - 243 hours)
248
-------
S!
- - . - _ 2/23/74
STATUS REPORT CF OPERATING CONCITICNS FC!;. INTEGRATED OPERATION OF S02 RECCVERY PROCESS
fO
-P-
:
ij
.1
!;!
4,
OPERATING PERIC3:
DATE: 2/23/74
GATE: 2/24/74
PRCCESS ELAPSED TIKE
P
LES
TIME CF RECCRC: Z3:15 'IRS TC Z4: 0
TIME CF RECCRC: 0: 0 .IRS TC 6:15
CF PERIOD: START 18il.CC HRS / END
HRS
HRS
-
.
243. CO HRS LENGTH CF PERICD: 55.00 HRS
FCR OPERATING PERICO:
->
!*
f'
l".
'"*
a
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--
IT
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3ti
S .
fa"
= s
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5 ,
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u
5 -'
-..
5
3"
S02 SCR8ER
2:15
6: 15
13:15
17:15
21:15
1: 15
5:15
2:15
6:15
13:15
17:15
2 1 : 1 5
1:15
5:15
23:15
6:15
.
1:15
9:15
17:15
1: 15
2:45
14: 2
3:15
12: 15
l: 2
5:15
19:15
4: 2
11:15
19:15
11:15
19:15
HRS
H.SS
HRS
H.RS
HRS
HSS
HRS
HRS
HRS
H^S
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS.
HSS
HSS
HRS
HR.S"
HRS
HRS
HSS
HRS
HRS
191.00
195. CC
226.00
23C.CO
234. CC
23S.CC
242. CC
A V E
191. CO
195. CO
226.00
23C.OO
234. CO
233. CC
242.00
A V E
188.00
243.00
A V E
19C.OO
195. CO
23C.CO
238. CO
A V c
191.50
2C2.30
216.00
225. CO
237.80
242.00
A V E
134. CO
192.20
2CC.CO
zee. co
316. CO
22''.. t3
Z32.CO
HRS
HRS
HRS
HRS
HRS"
HRS
R A
HRS
HRS
HRS
HRS
HRS
HRS
(ET)
(ET)
ItT)
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G E_s
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S02 CONC INLET FLUE G.'S
S02 CCNC INLET FLUE G"S
S02 CCNC INLET FLUE G/IS
S02 CCNC INLET FLUE G^S
S02 CCNC INLET FLUE G;>S
SC2 CCNC INLET FLUE G-1S
SC2 CCNC INLET FLUE C-,!S
S02 CCNC CUTLET FLUE £S
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SC2 CCNC CUTLET FLUE c;*s
S02 CCNC CUTLET FLUE S*S
H20 CCNC INLET FLUE G,!S
H20 CCNC INLET FLUE G..'S
H20 CCNC INLET FLUE G.SS
CRIFICE PRESSURE DRCP
CRIFICE PRESSURE CRCF
CRIFICE PRESSURE DRCP
CRIFICE PRESSURE CRCP
.CRIFICE PRESSURE DRCP
ORIFICE TEMPERATURE
CRIFICE TE'-'PERATtSc
CRIr.ICE TEKFERATLRE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
WEIGHT CYCLCNS CUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNS DUST
HEIGHT CYCLC.\£ CUST
WEIGHT. CYCLCSE OUST
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2/23/74 PAGE 3 ^
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INLET
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0.133
% (VCLUME) .
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/ Y200(4,T) =
/ Y2CCi4,T) =
/ Y200(4,T) -
/ Y200(4,T) =
/ AY2000 =
1K400
11.8-00
10.200
12.800
14.600
12.160
S (VCLUME)
S (VCLUME)
S (VCLUKE)
? (VCLUME)
? (VCLUMEI
S (VCLUKE)
..
^
:2
Z3
^
;«
(GS-206)
- (GS-2C6)
! GS-206)
(GS-2CC)
(GS-2CC )
(GS-2CO)
(GS-2CO)
5GS-20C)
(GS-2CC)
(GS-2CO)
/ Y2C6(4,I) -
/ Y206i4,Tl =
/ AY206C =
/ Y200(5,T) «
/ Y2CO!5tT) =
/ Y2CC(5tT) =
/ Y2CC!5,T! =
/ Y2CO(5,T) =
/ Y2CC(5,T! =
/ AY200E =
48.900
47.600
57.700
55.600
55.200
~ 56.700
55.300
54.2CC
55.7S3
S (VCLUME)
S (VCLUME)
S (VCLUME)
S (VCLUME)
? (VCLUME)
% (VCLUME)
* (VCLUME)
? (VCLUME!
S SVCLUME!
-^
~.
-O
JT'
-:
.1
»>
_.
(GS-2C6)
(GS-206)
(GS-206)
I G-2CC!
( G-2CC)
( G-2CC)
I G-2CO)
( G-2CO)
/ Y206(5,T) =
/ Y206!5,T) =
/ AY206E =
/ G2C3!5,T) =
/ G2QC(5,T) «
/ G200(5t7) =
/ G2CO!S,T) =
47.500
49.900
48.700
150.000
150. COO
150. COO
1 > 0 . 0 C G
150. 'COO
% (VCLUME)
S (VCLUME)
% (VCLUMEI
CFH (70 CEG F)
CFH i7C EEC F)
CFH !7C CcG Fi
CFH !7C D=G F)
CFH <7C CEG F)
*t
rf»
a
.,
-7
^
-\
-------
N>
Ui
U>
AVERAGE:
N2 INLET VCL FLOW RATE
< G-2CC) /
AG200E
2/23/74 PAGE 5
150.000 CFK (70 CEG F)
^
III
; I
7.
fte
K
P
fV
':>
IT
5:15
9:15
9:15
9:15
HRS
HRS
HRS
HRS
9:15 HRS
5:15
9: 15
9:15
5:15
9:15
9:15
HRS
HRS
HRS
HRS
HRS
194. CO
222. CC
246. CO
A V £
222.00
246.00
A V E
194. CO
222. CO
246.00
A V E
1S4.CO
222. CO
246. CO
A V E
HRS
HSS
HRS
R A
HRS
HRS
R A
HRS
"HRS
HRS
R A
HRS
HKS
HRS
R A
(ET)
(ET)
-------
Ul
r
;
ji
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t;
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t
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IT!
1
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j
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;
K
P
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pr
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23
?: fl
21:15
17:12
7 7- 3d
6:26
...2= 8
21:15
17:32
22:38
6:26
17:32
22:38
6:26
17:32
22:38
6:26
2:15
21:15
9:15
2:15
5: 15
HRS
HRS
HRS
LiO C
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
_H_S_S
HRS
HRS
HRS
HRS
19C.90 HRS
234. CO HRS
A V = R A
23C.30 HRS
3 2 e * n uo e
243.20 HSS
19C.VO HSS
234. GO H^.S
A V £ R A
23C. 30 HRS
235.40 H=S
243.20 HRS
AU "" O f
23C.30 HRS
235.40 HRS
243.20 HSS
A V E R A
23C.30 HRS
235.40 HRS
2^.2.20 1-RS
A V E R i
H 2
(ET)
(ET 1
G E :
(ET)
1 CT 1
(ET)
(ET)
(ET)
G E :
(ET)
(ET)
(ET)
Ge
(ET)
(ET)
(ET)
G E :
(ET)
(ET)
(ET)
G E :
191. CO HRS (ET)
21C.CC HRS
22Z.CO HRS
23. CO HSS
242. CO HRS
A V E R A
(ET)
IET)
(ET)
(ET)
G E :
S GENERATOF/SU
H2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H,2 CONC CUTLET GAS
H2 CONC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CONC CUTLET GAS
N2 CCNC INLET GAS
N2 CONC INLET GAS
N2 CCNC INLET GAS
N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
*' "> f*H R i" PI'Tl CT f" A C
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H.2S CONC CUTLET GAS
H2Q CCN'C CUTLET GAS
H2C CCNC CUTLET GAS
H20 CCNC CUTLET GiS
H20 CCNC CUTLET GAS
N2 INLET VCL FLOW RA"E:
N2 INLET VCL FLCh RATE-
N2 INLET VCL FLCV< RAT?
N2 INLET VCL FLCK RA~£
N2 INLET VCL FLCK RA7E:
N2 INLET VCL FLOW RATE
L F U R S
(GS-1CC)
(GS-1CCI
(GS-1CC)
(GS-108)
(GS-1CE )
IGS-lCt)
(GS-ICS)
5GS-1CC)
(GS-1CC)
IGS-1CC)
(GS-ICB!
(Gs-icei
SGS-ICE)
( G5-1C S i
IGS-106)
(GS-lOc)
(GS-lCc)
JGS-1CS!
IGS-108)
(GS-1C6)
(GS-ICo)
(ETI
IET)
(ET)
A L :
T E :
!ET!
(~T)
A L :
T E :
(ET)
(ET)
G £ :
:ETJ
G E :
HEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DLST
WEIGHT FILTER CUST
ViEIGHT FILTER CUST
WEIGHT FILTER CUST
WEIGHT FILTER CUST
3 TOT S CN CYCLCNE C";ST
* TOT S CN CYCLCNE 0:,ST
S TOT S CN CYCLCNE C'J-ST
% TCT S CN FILTHS D'J H
y TOT S CN FILTER O'J'ST
0-101)
C-1C1)
D-1C1 )
D-101)
( D-101)
{ D-101)
{ D-102)
( D-102)
t D-1C2)
( D-102!
1 D-1CIJ
( 0-101)
J D-ICi)
( D-1C2)
< C-1C2)
/ CD10KT)
/ CD10KT)
/ C010KT)
/ CD10KT)
/ V.'D1C1
/ RD1C1
/ CD1C2(T)
/ CC102!T)
/ W31C2
/ R0102
/ 010K1.T)
/ ElOUl.T)
/ AD101A
/ C102(1,T)
/ A0102A
=
=
ss
=:
=
=
=
=
=
0.0
0.176
0.322
0.263
0.761
0.014
0.0
0.0
0.0
0.0
31.600
30.700
31.150
0.0
0.0
LB CUST
LB CUST
LB CUST
LE CUST
L8 CUST
LB CUST/HR
L2 CUST
L2 CUST
LB CUST
LB CUST/HR
3 (WEIGHT)
S (HEIGHT)
?' UEIGHT)
% (V.EIGHT)
% (WEIGHT)
15
*!
H
^
^,
'4
}
-«
j
^
i
!.-!
-------
;
!
i
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*
T!
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iX
ii
j>
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n
3J
10 :J
Ol Is!
LJ
i -
u
?;
5:15 HRS 194.00 HRS (ET)
9:13 hRS 222.00 HRS (ET)
9:15 HRS 246.00 HRS (ET)
AVERAGE:
5:15 HRS 194. CO HRS (ET)
9:15 HRS 246. CC HRS (ET)
AVERAGE:
23:15 HRS 188. CO HRS (ET)
9:15 H*S 246.00 HRS (ET)
AVERAGE:
23:15 HRS 236.00 HRS (ET)
5:15 hRS 242. CO HRS
RATE
RATE
RATE
FUR C C t
CCLLECTE;
COLLECTS:
CCLLECTES
CCLLECTEC
CCLLECTEC
iCS- 9C) /
(CS- 90 /
ICS- 9C) /
(CS- 90) /
y
!,
M
i;
S
!"
I,
H
f>
b*
H
£<
ij
a
j
-T
y
*
' i
t
u
-------
2/23/7*
STATUS REPORT CF OPERATING CONDITIONS FCR INTEGRATED OPERATION OF S02 RECCVERV PROCESS
PAGE
NJ
Ul
j;
.
OPERATING PERIOD:
QiT = : 2/23/74 T1XE CF RECCRC
PROCESS ELAPSED TIME CF PER.ICO:
0: C rK
START 168..
": sitMKARY CF INTEGRATED PROCESS PERFORMANCE:
S
.:-
b
r *
r*
("'
i«
.V
1.
2.
3.
4.
S02 REMOVAL
H2S UTILIZATION
ACIO CONVERSION (TO SULF'JR)
1-2 UTILIZATION (TO H2S)
PRS02 =
PVCS *
PHCHS =
j
S TC 24: C HRS
I C 6s 1 5 rRS i
CC HRS / ENC 243.00 f-RS LENGTH OF PERICC: 55.00 HRS v
- - - i
T
, i
9
94.15 Z (ACTUAL) 90. C S (GCALI ,-t
'.,
9C.97 S (ACTUAL) 95. C J (GOAL) ;«
4
36.56 % (ACTUAL! 99.0 J (GOAL) W
rJ
72.29 % (ACTUAL) 90. C I (GOAL) - >J
r» §'
-
y
5.
6.
SULFUR RECOVERY
H2 UTILIZATION 4" UNIT
PRS
PUH2 =
63.38 % (ACTUAL) 1CO.O 1 (GOAL) OF SCRBEC SC2
18.34 Z (ACTUAL) 25. C S (GOAL) OF STRIPPED SL'LFUR a
93.53 % .-,
=» 71
i*:
"*;
r.
*
w
K
T;
i ;
7.
8.
5.
1C.
11.
RESIDUAL SULFUR ON CiRECN
CARBON RECYCLE RATE IDS)
ACIO LOADING INLET CAREON 6" UNIT
MOISTURE CCNTENT INLET CARBON 6" UNIT
ACID LOADING INLET CiRECN 8" UNIT
^ i?. nnrsTURF CCNTENT INLET CARBCN 8" UNIT
:i
3*
r"
U
"i
w
HI.
,
13.
14.
TOTAL AC'D CONVERTED 6" UNIT
SULFUR CONVERSION (TO K2S)
L">T Sill PLR TPNCENSER EFFICIENCY
X9CA =
RC90 =
X301C -
X301B »
X302C =
X302B =
PVC
PSCI-S =
ERV400=
fAJCR EVENTS CURING OPERATING PERICC:
SCIVED PRCBLEC ViITH OFF-GAS ANALYSIS FROM SUl
AT ENC CF PERICC LOWERED hYCRCGEN
C.C337 L8 S/L6 C w
29.922 LB C(DB)/HR . " jj
:J
C.256C LB ACIC/L8 C -:
^
C.C934 L8 H20/LB C s»
, !
C.256C LB ACIC/LB C rf
C.0934 LB H2C/LB C ^
?5.59 * ^
87.40 S p
1*5.58 S a
''
U
FJR GENERATOR J
FLOW RATH TO 120 CFH
-------
N)
STATUS RP.PCRT CF OPERATING CCNCtTICNS
OPERATING PSRIOC:
DATE: 2/23/74 TIME CF RECCRC: 23:
CATE: 2/26/74 TIME OF RECCRC: 0:
PRCCESS ELAPSED TIXE CF PERIOD: START
SULFUR MATERIAL BALANCE (USING PRCCESS H2S):
FCR INTEGRATED CPERATICN
IE t-RS TC
0 HRS TC
188. CO HRS
24: C
6: 15
~7~ENO
HRS
HRS
243. CO
2/23/74
CF S02 RECCVERY PROCESS
HRS
LENGTH OF PERIOD: 5
PAGE 9 ")
\
J
',.
:
S:00 HftS !.
1
' 1
..
p
;
r
E
tt
r
S 0 2
; N
INLET GAS AS S02
INLET C AS RESIDUAL S
TOTAL IN:
CUT
OUTLET GAS AS S02
CUTLET CARSON
CYCLCNE CUST
CCLLECTCR DUST
CiRECN WEEPAGE
TCTAL OUT:
6" DIA CARBO
s c: R B
( ',- l!i> I
( C- lit 1
t S i- 1 (i ) /
( c- i;:) /
( :> li.) /
< ':- i;:> /
(C'.- K'l /
/
R GEN
BC12A
SI300
BC201A
BD301A
S0300
ERA
3.5C93
3. 5093
3.
C.
3.
T C R
5093
0
'5C9~3
LS
LS
LB
LB
LB
SULFUS/HR
SU'LFUR/HR
SULFUR/HR
SULFUR/HR
S'JLrUR/HR
^
-'
-^
'.i
:.,
r.-.
^1
t1' '«.'
«;
ft!
Ai/
,7"
»S
I?1
K;
t N
INLET GAS AS H2S tCYL)
INLET GAS AS H2S (PRCC)
INLET CARBCN
TCTAL IN:
CUT
CUTLET GAS AS H2S
OUTLET GAS AS SC2
OUTLET CARBON
{ c-zc;.) /
< C-iCi ) /
t c-jc:. > /
-------
NJ
Ul
CO
1' *
i';
3]
'4,
V
'*
1
* '
r*
i?
»i
''i.
H 2 S
GENERATOR
I N
INLET CARECN
CUT
CUTLET
CLTL3T
CUTLET
CYCLCNE
FILTER
T
T C T
CA°.3CS
GAS AS
GAS AS
CUST
CUST
C T A
C
A L IN:
'
H2S
S
L CUT:
V E R A L L
( C-
1RV-
( C-
< G-
( C-
( 0-
(RV-
S L L
'SULFUR
C2)
'.CO
!.C3)
:.c^t)
id)
1C2)
:.cc>
F U
/ 3C202A
/ SHOO
/ SC103A
/ BG1048
/ SCIONS
/ BD101A
/ 8D102A
/ S0100
R 8 A
S T
=
_
C
s
-
S
9
9
1
7
1
C
0
R I P
.7849
.7849
.OC85
.6705
. 6 i C C
-C042
.0
= 10.2933
t A
N C
E
P E
L8
LE
L3
LE
LE
LS
LB
LS
2/23/74 PAGE 10
R
SULFUR/HR !>
SULFUR/HR i.
'Si
«.
SULFU'S/HR ';
SULFU3/HR ;,
SULFUR/HR iJ
SULFUR/HR I,,1
SULFUR/H.R Ijj
j
rfa f h
--
I N
-i INLET GAS 18"
t :
X
:r
-t
INLET G
CUT
CUTLET
CYCLCNE
AS 8"
GAS 18
CUST
UNIT AS SC2
UNIT AS CYL H2S
T C T A L
" UNIT AS SC2
13" UNIT
-.;. CCLLECTC3 DUST IS" UMT
=> CASECV XEErAGE 13" UMT
~ CYCLCNE CUST 6" UNIT
cv
~.
'x
??
S*
21
OUTLET
OUTLET
CUTLET
OUTLET
CYCLCN;
FILTER
«
GAS 8"
GAS 8"
GAS 4"
GA S 4 "
CUST
CUST 4
UNIT AS H2S.
UNIT AS SC2
UNIT AS H2S
UNIT AS S
4" UN: IT
" UNIT
TOTAL S
t 3-
S L t
I G-
( C-
( C-
(CV.-
( C-
( G-
( G-
( G-
1C)
F U
13)
Hf
121
i.21
,!C5)
:;c5 )
1C4 )
{ C-iOl!
! C-IC2)
U L P
U R
/ BG10A
/ BG201B
R I N
/ 8G13A
/ BDUA
/ S012A
/ BCK12A
/ EC 301 A
/ BG2Q58
/ BG2D5A
/ seiche
/ 8G104S
/ ED 101 A
/ HC102A
OUT
X.
=
=
=
;=
=
=
=
=
:
2
C
2
C
0
f*
c
0
0
0
c
1
0
2
.6933
.0
.6983
.1579
.~G170"
. CO 1 2
.0
.6331
.2359"
.C
.6100
.00<.2
.7253
IB
LE
LB
LS"
LE
L S"
IB
LB
LB
LS
LS
» P
LS
LB
','
SULFUR/HR '^
SULFUR/HR i,
SULFUR/r.R - . ''ri
...
SULFUR/HR 7i
SULFUR/HR T<
SULFUR/HR aj
SULFUR/HR " W
SULFUR/H3 V
SULFUR/HR :i
SULrUR/HS . -j
SULFUR/HR '
SL'LF^R/HR ,.
SliLFUR/i-S :-
SULFUR/HR ^
B?
3* 3«(
^
1
^i
,.
j*
», **
"5
«;
rt-
-------
2/23/74
PAGE 11
hVCRCGEN MATERIAL BALANCE:
t[
I*
',.
'L
! N
S U L F
INLET GAS AS H2
i_ INLET GAS AS H2S (CYL)
f .
i
*.-
»
INLET GAS AS H2S (PRCC)
INLET GAS AS 1-20
INLET Ci'KSCN
T C
T A L IN:
UR GENERATC
! G-rC3) /
{ 6-ZC3> /
' BG203C =
' BG203B =
1 G-l':3) / EG203 =
( G-rOS! / BG203D =
( c-?/:i) / ec2o\ir =
(RV-::CO /
' H20C =
R
0.
c.
c.
c.
0.
1.
C09/
0 "
4793
1663
4S67
1420
LB
"LB"
LS"
Le
LE
LE
HYCRC-GEN/f-R
HYCRCGEN/hR
HY:RCG=N/HR
HYCRC5E.M/HR
'='
.
:
.;
>
9
CUT
:i
,j
5
:--.
-.:
ts_"i "^
in -*-
VQ '"'
W
*»
!*
;-i
OUTLET
OUTLET
CUTLET
CUTLET
T
I N
INLET
I'iLET
CUT
OUTLET
CUTLET
CUTLET
T
GAS
GAS
GAS
AS H2
AS H2S
AS H2C
CAR3CN
C T
H 2
GAS
A L CUT:
S GENERA
AS HZ
CAR3CN
T C
GAS
GAS
GAS
C T
T A U IN:
AS 1-2
AS (-2S
AS h20
A .L CUT:
{ G-:.:-:5> /
( G-::I:SJ i
f G-.1 :s ) i
\ C-2C2) /
!RV--1CC) 1
T C R / 3 U
1 G-l'3) >
! c-?:: ) >
(Rv-t:ci /
i G-I:«) /
{ G-i;^) /
IRV-ICC) y
' BG2C5C =
' EG205H =
' EG205C =
' SC2C2r =
' 1-C20C =
L F Li R
' BG103C =
' BC202H =
' HI IOC =
' BG104C =
' BG104H =
' BG104D =
' i-OiOO =
0.
r\ ^
C
^
U
0.
S T R
C.
C.
C.
0.
0.
r>
* *
0.
0023
C43C
O 7 c £
0 2 19
9025
I P
6630
0219
6C49
0093
4 793
1934
6624
LB
LE
LB
i- £?
P E
LE
LE
LE
L8
"LE"
LE
LE
HYCRCGcN/HR
HYCRCGEN/HR
hYCRCGEN/r-R
HYCRCGEN/I-R
R
HYCSCGEN/hR
HYCRCGS^/t-R
HYCRCGEN/KR
HYCRCGEN/hR
HYCRCGEN/hR'
HYERCGEM/VR
HYCRCGEM/rR
&
>
-
a
^
T;
~3
-t.
.
--
;,
-,
JO
-
i*1 ' K
?J
i
*
-------
APPENDIX A-12-2
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-1-5 (246 - 262 hours)
260
-------
2/26/73
PAGE 1
Ni
STATUS REPORT CF OPERATING CONDITIONS FOR INTEGRATED OPERATION CF soz RECOVERY PROCESS
(:>.
i.-i
i.i
V
v
i''
OPERATING PEPICO:
CftTE: 2/26/73 TIKE OF RECCRC: " 9:15 h>< TC 24: 0
CATE: 2/27/73 TIME OF RECCRC: 0: 0 h-.S TC 9:15
PROCESS ELAPSEC TIPE
CF PERICD: START 246 .CO HRS / END
HRS
HRS
270.
: 't
i'!
,,l
CO HRS LENGTH GF PERIOD: 24.00 HRS :.l
PROCESS VARIABLES FCR OPERATING PERICD:
h
i
~y.
'« ^
>r
is
M
'r
.i*
72
=3
"I
"""
W
~i
\"
r*
'
j.
1 ^
r"
'4i
r '
'.^
^
13:15 HRS
18: 2 HRS
21:15 HR S
l: 15 H.RS
5:15 HRS
13:15 HRS
19: 2 HRS
21:15 HRS
1:15 HRS
5:15 H.RS
21:15 HRS
13:15 HRS
22:15 HSS
6:15 rRS
13:15 HRS
22:15 HRS
6:15 HRS
11:15 V-RS
3:15 HRS
11:15 HRS
3: 15 HRS
16:15 HRS
0:15 H.RS
25C.OO HRS (ET)
254. SD HRS (ST)
25c.CC r 3 S ( C T )
262. CO HRS (ET)
266.00 H?.S
267. CO j-'S (ET!
AVERAGE:
243. CO HRS (£T)
254.00 H=.S (ET)
T C T A L :
S i T E :
243. :C r?S (ET)
264. CD !--. S IcT)
T G T 4 L :
RATE:
253. CO HRS (ET)
261.00 HRS (ET)
TOTAL:
5. - T E :
S 0 2 3 C R
S02 CCNC INLET FLLE G*3
S02 CCN'C INLET FLUE G/3
S02 CGNC IN-Lci FLUc Gti
S02 CCNC I.NLET FLLE GAS
S02 CCNC INLET FLUE G«S
S32 CCNC INLET FLUE G«S
S02 CCfiC CUTLET FLUE G4S
S02 CCNC CUTLET FLUE G«<
S02 CONC CUTLET FLUE G££
S02 CCNC CUTLET FLUE GAS
S02 CCNC CUTLET FLLE G*£
S02 CCNC CUTLET FLUE Gi£
H20 CCNC INLET FLUE G/S
H20 CCNC I.NLET FLUE G-
1CX-
(Ci*-
10) /
10) /
1C ! /
10) /
1C 1 /
10) /
16) /
16) /
16 ) /
16) /
16! /
10) /
10) /
1C! /
10) /
10) /
1C) /
1C ) /
1C! /
10 ; /
1C ) /'
IT * /
L t 1
11) /
11 !/
11! /
12 ) /
12) /
12 ) /
12) /
12! /
12) /
_-2.l./.
Y 10 ( 1 T T ) =
Y10(1,T) =
10 ( 1 » T )
YlO(ltT) =
YlOIltT) =
AY10A =
Y16!1,T) =
Y16!1,T) =
Y16U,T) =
Y16! 1 f T ) =
Y16(1,T) =
Y 1 0 ! 4 1 T i =
AY10C =
CPiOIT) =
C? 10 IT) =
DPIO'.T) =
SOP10 =
TL10(T! =
TLlO'Ti =
TLIC;T) =
A 7 L 1 C =
COU(T) =
CC11 IT! =
^D! 1 =
CC121T) =
C012!T) =
K012 =
RD12 »
CVJ12 (T ! =
V.'C'
9. £00 S (VCLU'ME) t=
9.SOO S iVCLUri = ) ~:
-,-
2.400 INCHES H20 ..;
2.400 INCHES H20 ..
2.250 INCHES H20 ;,:
2.383 INCHES H20 -j
ES
2C7.000 CFG c r.
30?,. COO CSG r
203. COC CHC F
2C4.333 CEG F ;,
,
0.0 LE CUST ;
4.200 L? C'JST
4.2".'0 LE COST
o..c£2 Lr :JST/HR
-1
C.O Li CUST
2.700 L= CUST ' .,
2.700 is :usr ' ' ,
0.169 IB CUSI /HR
C.O Lc CUST ,:
O.C54 LZ CUST ,,
O.C56 LE CUST .]
O.COV LS CUST/HR
;,
11:15 HRS 2-3.CO HRS iET)
S TGT S CN CYCLCNE 2LST
C- II) / C1K1.T) =
7.0feO ? (HEIGHT)
-------
N>
AVERAGE :
._5_HAS C._0 2_N R S_l £ Tl
A V ~E R A G E :
S TOT S CN CYCLCiNE
_?_TPLJL_CN_CC|-LECTQR_ CI S L
x TOT s CN cciVecTOR "ci.sr
< D- 11) /
I D- 12) / C12U.T)
2/2f/73 PAGE 2
7.0cO t (WEIGHT)
7.060 X (HEIGHT)
< D- 12) /
A012* =
_
7. "080
U EIGHT)
-------
to
i
I 6" 0 I A
v 17:15 HRS 254.00 HRS ( ET ) ? TOT
pi 1:15 HRS 262. CO HRS (ET) S TOT
i'j 5:15 HRS 266.00 HRS (ET) % TOT
|'L_ AVERAGE:* TOT
'*!
!'i 17:15 HRS 254. CO HRS (ET) % H20
: 1:15 HS.S 262. CO HP.S 1ET) 1 H20
iri 5:15 HRS 266. CC HRS (ET) t H2C
!«! AVERAGE:? H20
f» 9:15 HRS 246.00 HRS (ET ) WElGt-T
'> 9:15 HRS 27C.CO HRS ( ET ) WEIGHT
«! TOTAL: WEIGHT
»i RATE: V.EIGHT
U: 9:15 HRS 27C.OO HRS tET) S TOT
}*' . A V E R A G E : % TOT
!«
-«
t".
C7
&
u
C A R 8 O. K PR
S ON I\'LET CAR8CN
S CN INLET CAPSCN
S CN INLET CAPECN
S CN INLET CAHeCiV
CN INLET CARBCN
CN INLET CARBCN
CN INLET CARECN
ON INLET CAR8CN
CYCLCNE OUST
CYCLCNE OUST
CYCLCNE OLST
CYCLCNc CUST
S CN CYCLCNE DUST
S CN CYCLONE CLST
E C 0 N C I
CS-301 )
(CS-3C1)
fCS-301 1
(CS-301)
(CS-301)
(CS-301 )
(CS-301)
(CS-301 )
( 0-301)
( 0-301)
« D-3C1)
{ D-301)
( 0-301)
( 0-301)
T
/
/
/
/
"/
/
r
/
i
/
/
i
i
i
t 0 N c R
Z301U.T) =
Z30K1.T) =
Z3GHltT) =
AZ301A = .
Z301I2tT) =
Z30K2.T) =
7 3O 1 I ? . T 1 ~
AZ301B =
C030KT) -
CD30KT) =
WD301 =
RD301 =
0301(1. T) =
A0301A =
2/26/73 PAGE 3
8.440 t (V.EIGHT)
7.600 * (WEIGHT)
8.560 ? (WEIGHT)
8.200 * ( HEIGHT)
7.790 3 (HEIGHT)
7.460 3 (ViEIGKT)
6.790 % (V,EIGHT)
7.347 S (hEIGHT)
0.0 LB CUST
0.0 LB CUST
0.0 L3 CUST
0.0 L3 CUST/HR
0.0 S (WEIGHT)
0.0 S (KEIGrT)
-
'.
:
t
,';
--.
7J
,'4
r*
-*
...
-i
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-2
13
-*
H '
fc! -.
1 :
f> '>
P
-
13
HI
pi
(-(-._.
P
C-
I-!
Ij "
,
-,
-,
_;
t.
i '
-i
-------
2/26/73
PAGE
to
SULFUR
GENERATOR
1,4:45 HRS
23: 2 HRS
12:32 HRS
0:15 HRS
i 14:45 HRS
E
12:32 HRS
' 0:15 HRS
i
n
I 14:45 HRS
23:26 HRS
i
12-32 HRS
: 0:15 HRS
14:45 HRS
i 23:26 HRS
'
12:32 HRS
0:15 HRS
14:45 HRS
23:26 HRS
9:15 HRS
9:15 HRS
21: 15 HRS
21:15 HRS
21:15 HRS
21: 15 HRS
9:15 HRS
17! 15 HRS
1:15 HRS
5:15 HRS
251.50 HRS (ET)
259.80 HRS (ET)
AVERAGE :
249.30 HRS (ET)
261. CO HRS iET)
AVERAGE:
251.50 HRS (ET)
6C.20 HRS (ET)
AVERAGE:
249.30 HRS ( ET )
261.00 hRS (ET)
AVERAGE :
251.50 HRS (ET)
26C.20 HRS (ET)
AVERAGE:
249.30 HRS (ET)
261. CO HRS (ET)
AVERAGE:
251.50 HRS (ET)
26C.20 HRS (ET)
AVERAGE :
249.30 HRS ( ET )
261. CO HRS (ET)
AVERAGE:
251.50 HRS (ET)
26C.20 HRS (ET)
AVERAGE:
246.00 HRS (ET)
27C.CO HRS (ET)
AVERAGE:
253. CO HRS (ET)
AVERAGE:
253.00 HRS tET)
AVERAGE:
258.00 HRS !ET)
AVERAGE:
258.00 HRS (£T)
AVERAGE:
246.00 HRS (ET)
254.00 HRS (ET)
262. CO H?S IcT)
266. CO HRS i£T)
AVERAGE :
S02 CONC CUTLET GAS
SC2 CONC CUTLET GAS
S02 CCNC CUTLET GAS
H2S CONC INLET GAS
H2S CONC .INLET GAS
H2S CONC INLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CGNC CUTLET GAS
H2 CONC INLET GAS
H2 CONC INLET CAS
H2 CONC INLET GAS
H2 CCNC CUTLET GAS
H2 CON'C CUTLET GAS
H2 CCNC CUTLET GAS
H2C CCNC INLET GAS
H20 CCNC INLET GAS
H20 CONC INLET GAS
H20 CCNC CUTLET GAS
H2C CONC CUTLET GAS
H20 CCNC CUTLET GAS
N2 CQNC INLET GAS -
N2 CONC INLET GAS
N2 CONC INLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
M2 CONC CUTLET GAS
N2 INLET VCL FLOW RA'fg
N2 INLET VCL FLOVi RATE
N2 INLET VCL FLCVi RATE
Z TOT S ON INLET CA3'3Ch
% TOT S CN IN'LET CASeC!'.
S TOT S CN CUTLET CA16CN
Z TOT S CN CUTLET C«ECJ(
% H20 ON INLET CARBC-i
S H20 ON INLET CARBCV
% H20 ON CUTLET CAF-ECN
? H20 QK CUTLET CARECN
% ACIC ON CUTLET CAR2C!*
% ACID ON CUTLET G£R!=C:>
% ACID CN CUTLET CAREC.t
% iCIC ON CUTLET CA3ECA
% ACID ON CUTLET CARHCN
(GS-206) /
(GS-206) /
(CS-2C6! /
(GS-2CC) /
(GS-200) /
CGS-200) /
(GS-206) /
(GS-2C6) /
(GS-206) /
(GS-2CO) /
(GS-2CO) /
(GS-2CO) /
(GS-2C6) /
«GS-2C6) /
(GS-206) /
(GS-2CC) /
(GS-200) /
«GS-200> /
IGS-206) /
(GS-206) /
(GS-2C6) /
CGS-2CO) /
(GS-200) /
(GS-2CO) /
(GS-206) /
(GS-206) /
(GS-2C6) /
( G-2CO) /
< G-200) /
< C 2CO) /
(CS-302! /
(CS-302) /
1CS-2CO) /
(CS-2CO) /
(CS-302) /
(CS-302) /
JCS-2CO) /
{CS-2CO! /
(CS-2CC) /
JCS-2CO) /
(CS-2CO) /
1CS-2CO) /
(CS-2CC) /
Y2C6(ltT) =
Y206IltT) =
AY206A =
Y200(2tT) =
Y200(2iT) =
AY200B "
Y206(2,T) =
Y206(2»T) =
AY206E =
Y200(3,T) =
Y2CC(3tT) =
AY200C =
Y206(3tT) =
Y2060.T) =
AY206C =
Y2CC(4,T) =
Y2COI4.T) =
AY200C =
Y206(4,T) =
Y206(4,T) =
AY206D =
Y200(5,T) =
Y20C(5,T! =
AY20CE =
Y206(5tT) =
Y2C6C5»T! =
AY2G6E =
G20C<;,T) =
G2CO(5,T) =
AG2COE =
Z302(UT) =
AZ3C2A =
220C(1,T) =
AZ20C* =
Z3C2I2.T) =
AZ302B =
2200(2, T) =
AZ200E =
Z2C013,T ) =
Z200I3.T) =
Z^OCOrT) =
Z2CCi3, 5 i *
AZ2CCC =
0.960
1.100
1.030
28.300
25.700
27.000
1.000
0.720
0.860
0.0
0.0
0.0
0.0
0.0
0.0
10.200
11.200
10.700
48.300
48.200
43.250
58.900
58.500
58.700
49.500
49.800
.49.650
180.000
180.000
180.000
8.200
B.200
24.000
24.000
7.350
7.350
0.240
0.240
0.940
1.210
1.310
i.iJC
1.140
? (VCLUHE)
* 1 VCLUME I
* (VCLUKE)
* (VCLUME)
X (VCLUME)
T (VCLUME)
% (VCLUME)
? (VCLUME)
S (VCLUME)
1 (VCLUME)
* { VCLUME )
? (VCLUME)
% (VCLUKE1
* ! VCLUM E )
S (VCLUME)
S (VCLUME) ' -
? (VCLUME!
? (VCLUME)
? (VCLUME)
S. (VCLUME)
S (VCLUME)
? (VCLUME)
S (VCLUME)
S (VCLUME)
* (VCLUME)
? (VCLUME)
Z (VCLUHE)
CFH (7C CEG F)
CFH (70 DEC F)
CFH (70 CEG F)
? (WEIGHT)
? (HEIGHT)
? (V,EIC-nT)
S {V.£!GrT)
J (V.EIGHT)
% (WEIGHT)
S (WEIGHT)
.3 (XE:C-:-.TJ
" (WEIGHT)
? (WEIGHT)
% CnEIGHTJ
k ! ? t i u r T )
? (WEIGHT)
j
t'
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1 1
i .
3.
ill
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73
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-^
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-
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.-
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.-
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-
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-------
2/26/73
PAGE
H 2 S
GENERATOR /SULFUR
STRIPPER
Si
ON
Cn
V
Ij
Jt
4" '
i!
i*!
I-.
v
>l
>!
:»
R
H
r-
*
7.'
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f'i
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H
Li
P
P
P
y
P
P
i.
i**
iJ
.,
<...
..
.11: 8 HRS
15: 8 HRS
" 1:26 HRS
12:32 HRS
0:15 HRS
11: 8 HRS.
15: 8 HRS
1:26 HRS
12:32 HRS
0:15 H°.S
12:32 HRS
0: 15 hRS
12:32 HRS
0:15 HRS
13:15 HRS
19:15 H«S
1S15 HRS
12:15 HRS
16:15 H?.S
20:15 HRS
0:15 HRS
4:15 HRS
9M5 HRS
9:15 HRS
3:15 HRS
21:15 HRS
247.90 HRS tET)
251.90 HRS 1ET)
262.20 HRS (ET)
AVERAGE:
249.30 HRS (ET)
261.00 HRS (ET)
AVERAGE:
247.90 HRS (ET)
251.90 HRS (ET)
262.20 HRS tET)
AVERAGE:
249.30 HRS (ET)
261. CO HRS (ET)
'- V E R A G E :
249.30 HRS (ET)
261. CO HRS (ET)
AVERAGE:
249.30 HRS (ET)
261. CO HRS (ET)
AVERAGE :
25C.CO HSS -ET)
256. OC HRS (ET)
262. CO HRS IET)
AVERAGE:
249. CO HRS (ET)
253. CO HRS (ET)
257. CO HSS !ET)
261. CO HRS (ET)
265.00 HRS (ET)
TOTAL:
RATE:
246. CO HRS IET)
27C.CO HRS <£T)
TOTAL:
RATE:
C.O HRS (ET)
AVERAGE:
258.00 HRS (ET)
AVERAGE:
H2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CONC INLET GAS
H2 .CONC INLET GAS
"
H2 CONC OUTLET GAS
H2 CCNC CUTLET GAS
H2 CONC OUTLET GAS
M2 CCNC INLET GAS
N2 CONC INLET GAS
N2 CONC INLET GAS
N2 CCNC INLET GAS
N2 CQNC CUTLET GAS
N2 CCNC CUTLET GAS
N2 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CONC CUTLET GAS
H2S CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CONC CUTLET GAS
H20 CCNC CUTLET GAS
N2 IKLET VCL FLOW RATE
N2 INLET VCL FLCW RATE
N2 INLET VCL FLOW RATE
N2 INLET VCL FLCW RATE
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CCST
WEIGHT CYCLCNE CC'ST
WEIGHT CYCLCNE CCST
WEIGHT CYCLCNE OUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CUST
WEIGHT FILTER CUST
WEIGHT FILTER CUST
WEIGHT KILTER CCST
HEIGHT FILTER CUST
% TOT S ON CYCLCNE CCST
% TOT S CN CYCLCNE CUST
X TOT S ON FILTER OLST
% TOT S CN FILTER CLST
,,
58.000 ? (VCLUHS)
57.133 t (VCLUME) . :t
53.900 ? (VCLUHE) :j
53.500 ? (VCLUHE) ;:»
58.700 31 (VCLUHE)
Sji
28.300 ? (VCLUME) -.'
25.700 ? ( VCLUME) -
27.000 S (VCLUME) ' W
10.200 ? (VCLUNE)
11.200 S (VCLUKE) i,
10.700 ? (VCLUME) .-,
175.000 CFH (7C CEG F) :'*
175.000 CFH (7C CEG F) :-|
175.000 CFH (7C DEG f) -,
175.000 CFH (70 CEG F) ^
.,'
0.0 LB CUST
0.055 LB CUST :-3
0.070 L6 CUST - y
0.064 LB CUST i.'
0.066 LB CC'ST (J
0.255 L6 CUST -J
0:016 IS CUST/HR
0.0 LE CUST ^
0.0 LB CUST 0
0.0 LE CUST
0.0 LB CUST/HR ^
24.000 ? (WEIGHT) L!'
24.000 I (WEIGHT) d
^
24.000 ? (WEIGHT)
24.000 ? (WEIGHT) ' - :;
'2
bi
..,
- 1
if
-------
2/26/73
PAGE
CARBON
ON
k 21:_15 HRS 258. CO HRS t ET ) S RESICUAL S CN CARBCf.
'. AVERAGE:* RES 1C
'' 21:15 HRS 258. CO HRS
UAL 3 C
UAL H2C
L'AL_H2C
RECYCLE
RECYCLE
S U L
N CARBC;,
CN CAR-r:N
ON CAR !CI*
RATE
RATE
FUR CON
-i
5* -
'
** . a
bo »
3:
p*
bi
^
r*
-------
2/2e/73
STATUS REPORT CF OPERATING CONDITION'S FCR INTEGRATED OPERATION OF S02 RECCVERY PROCESS
hJ
i
_
i.
OPERATING FiRISD:
CATE: 2/26/73 TIME CF RECCRC
CAT£: 2/27/73 TIME OF RECCRC
PRCCESS ELAPSED TIKE CF PERIOD:
: 9:15
: 0: C
H*J TC 24: 0 HRS
H3S TO 9:15 HRS
,
s
START 246. (C hRS / END 270.00 f-RS LENGTH CF PERIOD: 24.00 HRS
SLyfiRY CF INTEGRATED PRCCESS PERFORMANCE:
S02 REHCVAL.
PRS02 =
S3. 71 X (ACTUAL) 90.0 % (GCAL)
I
^
'.
r ' ::
1 *
- 3.
i
- 4.
3
*: 5.
= 6.
rs
7.
r~\
3.
» 9.
H2S UTILIZATION
ACID COVERSICN (TO SULFUR)
H2 LTILIZiTICN (TO H2S)
SULFUR RECOVERY
t-2 UTILIZATION 4" UNIT
RESIDUAL SULFUR ON CARBON
CiRSCN RECYCLE RATE (28)
ACID LCACING INLET Ci.ReCN 6" UNIT
--' 10. fOISTURc 'CONTENT INLET CARSON fc" UNIT
i- 11.
al 1?.
13.
14.
» 15.
r1 '
,
'2
*;
ACID LCiC!V3 INLST CiRECN 3" UNIT
_fOI.STURr *CNTENT_ INLET CARBON 8" UNIT
TOTAL ACIC CONVERTED 8" UNIT
SL'LCL-S CCNVEKSiO'.1 (TO H2S)
SULFLR CCNCENSER EFFICIENCY
V4JCR EVENTS DURING CPERATIMG PERIOD:
iT START OF PERIOD CUT h2 FLOVi TO
FUV2S »
PVCS -
FhCKS =
PRS =
PUH2 =
X90A =
RC90 =
X301C =
X3018 =
X302C =
X3023 =
PVC =
PSCHS =
£R\'4CO =
120 CF!-.
96.23 * (ACTUAL) 95. C * (GCAL)
87.96 5 (ACTUAL; 99.0 $ ;GCALI
69.39 S (ACTUAL) 90. C * (GCAL)
77.43 Z (ACTUAL! 100.0 % (GOAL) CF SCR8EO SQ2
21.64 % (ACTUAL) 25.0 * (GOAL) OF STRIPPED SULFUR
ICO. CO Z
C.C331 L8 S/L5 C
;:9.91S LB C1CB1/HR
0.2453 L3 ACIC/ie C
(i.lC14 LB S2C/LS C
c.2453 Lb ;::C/LS c
C.1C14 LB H2C/L6 C
93. SC %
77.72 S
97.14 S
FRC!' 132 CFH
-
-
r
*;!
-;
:i
14
"5
J
'-J
-^
'-=
^
;s
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3
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t.
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-
-------
2/26/73
STATUS REPORT CF OPERATING CONDITIONS FCP. INTEGRATED OPERATION OF S02 RECOVERY PRCCESS
PAGE S
OPERATING PERIOD:
_EALE_: 2X 2 6 /13_
_CAT£: 2/2.7/73_
jrjM£ OF RECORD: 9:15 MRS. TO 24: 0 HRS
TIKE OF RECORD: 0: 0 t.RS TG 9:15 HRS
PRCCESS ELAPSE^..TIX-E CF PERIOD: S_TART__2't( .CC HRS /gNC 2'70.CO"t-_RS LE-NC-TH CF PERIOD; 24.00 HRS
SULFUR MATERIAL 6A(.ANCE (USING PRCCESS H2S1:
S 0 2
_S C R S E R
I N
INLET GAS _A_S_S02
t G- 13) / BG10A =
2.5609 LE SULFUR/HR
N>
CT>
00
I
1
t
\
i
;
.
c
i
1
j
I
,.
I
I
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t
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3
INLET C AS RESIDUAL
TOTAL
CUT
OUTLET GAS AS SC2
CUTLET CARBON
CYCLONE OUST
COLLECTOR DUST
CARSON hEEPAGE
TOTAL 0
6" D I A
I N
INLET CARBON
TOTAL
CUT
OUTLET CARBON
CYCLCNE OUST
TOTAL C
I N
S ( C- 1 1 i I
I N : (RV- 1C) i
{ G- 13 ,
( C- 12 t i
< 0- 111 i
< C- 12) i
(Cfe- 121 -
U T : (RV- 1C!' i
CARBON PR
t C- 12i .
I N' : ,
U T : (RV-3CCI i
SULFUR G 1: I
,
' BC11A =
' SI10 =
r BG13A =
' 8C12A =
' BD11A =
' BD12A «
f BCU12A <
' S010 =
E C 0 N D I T
I BC12A «
' SI 300 =
1 BC201A =
f BD301A =
t SO 300 =
i E R A T C R
C.?8B9
3.5498
0.1610
3.3849
O.C186
C.CU9
O.CC08
3.5772
I 0 N E
3.3849
3.3649
3.3849
0.0
3.3849
LS
L6
LS
LE
LE
L8
LE
LE
R
LE
LS
LE
L8
LB
SULFUR/HR
SULFUR/H3
SULFUR/HR " - ?
SULFUR/HR -.:
SULFUR/FR r
SULFUR/HR -,
SULFUR/HR . r
a
3
SULFU3/HR :
SULFUR/HR - -
-^
SULFUR/HR -
SULFUR/HR a
SULFUR/HR -
«
,
-:
IMLET GAS AS H2S (CYL)
INLET GAS AS H2S (PRCC)
_^ '- EI_CIR_B ON
T C T A L
1 N ;
{ G-2C1I / SG201B
< G-2C1i / BG203R *
J_<>2C 1 I_/_BC201 A '
(RV-2CCI / SI200 =
6.6729 L* SULFUR/HR
__3.3349_LB_SULFUR/hR_
10.0579 LE SULFUR/HR
CUT
OUTLET GAS AS t-2S
OUTLET GAS AS SC2
CUTLET CAR3C.N
T C A L
OUT
( G-2C5 I / BG205B =
( G-2C5 i / 3C-20SA =
_L_C- 2 C 2_)_/_B C 2 0 2A_y
(RV-2CC I / ~S0200 =
0.2513 L2 SULFUR/HR
C.3010 LE SUS-FUR/hR
9.5749 LB SULFJR/i-R
10.T271 L"e SULFUP'/HR
-------
2/26/73
PAGE
H 2 S
GENERA -TOR
FUR
STRIPPER
1;
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s'
.
':
i
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T,
r
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1 N
INLET CAR8CN
T C T A L IN:
CUT
OLTLET CARBON
OUTLET GAS AS H2S
CUTLET GAS AS S
CYCLCNE CUST
FILTES CUST
TCTAL OUT:
OVERALL
I N
INLET GAS 18" UNIT AS SC2
INLET GAS 8" UNIT AS CYL H2S
TOTAL
CUT
OUTLET GAS 18" UNIT AS SC2
CYCLCNE CUST 18" UNIT
COLLECTOR DUST 18" UNIT
CARBCN ViEEPAGE 18" UNIT
CYCLCNE CUST 6" UNIT
CUTLET GAS 8" LNIT AS H2S
CUTLET GAS 8" UNIT AS SC2
OUTLET GAS 4" UNIT AS K2S
CUTLET GAS 4" UNIT AS S
CYCLCNE DUST 4" UNIT
FILTER CUST 4" UNIT
TOTAL S
.
{ C-.1C2)
(RV-iC C)
( C--.C3)
I G-U4!
< G--C4!
< C-U.1)
( C-U21
(RV-iCC)
S t L 1 U
1 G- 1CI
( G-2C1I
s u L r u
( G- !3)
< D- 11)
« C- 12)
(CV.- 12)
t C-3C1)
G-2C5)
G-2C5)
G-K4)
G-K4)
D-1C1)
0-1C2)
U L F I A
/ BC202A
/ snoo
/ SC103A
/ 6G104E
/ SC-.104S
/ eoioiA
/ BD102A
/ S0100
R B A
/ BG10A
/ 8G201B
R I N
/ BG13A
/ SOUS
/ 8012A
/ ECW12A
/ E0301A
/ BG205B
/ 8G205A
/ BG1046
/ BG104S
/ BD101A
/ B0102A
OUT
=
:s
=:
Si
=
=
L A
-
:
s
s
3
^
S
X
=
=
:
9.5749
9.5749
C.9889
6.6729
1.8583
O.CC38
0.0
9.5240
N C E
2.5609
0.0
2.5609
0.1610
C.0186
0.0119
0.0008
0.0
0.2513
0.3010
0.0
1.85S3
0.0038
0.0
2.6067
LE
LB
LB
LE
LB
LB
LS
LB
LB
LB
LE
LE
LB
LB
LB
LB
LE
LB
LB
LB
LB
LB
LB
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULrUR/H.R
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/H.R
SULFUR/HR
SULFUR/hR
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/H.R
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/KR
SULFUR/HR
SULFUR/HR
SULFUR/HR
-
'.
i
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r
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't
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-5
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1 1
'.!
I-' .
'»;
(i
. I
i-
i"
u:
HYDRCGEN ."ATE3IAL BALANCE:
I N
INLET
IXLET
INLET
i^LET
S U
GAS AS H2
GAS AS I-2S (CYL)
GAS AS H2S (PRCC)
GAS AS r20
CAR3CS
TCTAL I N
L F I/ R i; 6
( G-2C3)
*< C-2C3)
! G-2C3)
( C-2:3)
', c-2;u
: IR\-2CC)
N 6 R /» T C
/ 3G2C3C =
/ BG2C3B =
/ 8G203 =
/ BC-2030 =
.' BC2Clh =
/ HI2CO =
R
C.O
c.o
0.4170
C-U52
C.4869
1.0691
LE
L2
t- r- r-
ru ru m
LS
2/26/73 PAGE 10
HYCRCGEN/HR
HYCRCGEN/hR
HYCRCGEN/HR
HYCnCGEN/r-R
HYCRCGEN/rR
HYCRCGEN/r-.S
i^
j)
:,
.
i'
-,'
';! .,'
?' CUT t»
r-
1
f1!
1.'
p
DLTLcT
Ci.;TLeT
OLTLcT
OUTLET
T
GAS AS H2
G1S AS H2S
GAS AS K20
CARBON
C T A L OUT
H 2 S GENE
{ C.-2C5)
. I C-2C5)
( C-2C5)
( 02:2)
: (RV-aiC)
R A T C f. / S
/ BG205C =
/ EG205h =
/ SG205D =
/ 8C202H. =
/ K12CC =
U L F U R
C.C
0.0157
C . S S C 9
0.0199
0.9166
STRIP
L8
LE
LS
LE
LB
P
hYCRCGSN/HR
KYCRCGEN/KR
HYCRCGEN/HR
hYCRCGEN/HR
HYCRCGEN/HR
E R
t
^
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:*
73
* i N y
n
i
P
i.
£,'
i,'
H
ta
ES '
INLET
If.'LET
CUT
CLTLET
CL'TLET
CLTLET
1
GAS AS H2
CARSCN
TCTAL IN
GAS AS H2
GAS AS M2.S
GAS AS H20
C T A L OUT
< U-II3)
< C-2C2)
: (R'/-i:C)
C r,- 1 C4 J
( G-IC'V)
( G-IC4)
: ..; (R'/-1CC)
/ EG103C «
/ 8C202*- =
f nice =
/ EGIC4C =
/ EGlO^h =
/ BG.104D =
/ H01CO =
C.6C09
0.0199
0.6208
C.O
C.4170
C.1652
C.5822
LE
LE
LE
LB
LE
LH
Lfi
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HS
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/H.R
^
-4
1
-%
n
U.'
»'
rr
a
^
Si
=.' y
*_! ' -j
H ' ^
»j> ijc
'*' ~"
:_, ' -:
ij
I ' ' - " - -
-
1*
-.
UV
-------
APPENDIX A-12-3
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-6 (37 - 51 hours)
271
-------
4/21/74
STATUS REPORT CF OPERATING CONDITIONS FOR 'NfEGRATEQ CPER4TICN CF SC2 RECCVERY PROCESS
PAGE 1
C?E"-
Q
3
j|
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0
I-'
(4
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S02SCRBER -7
16: 2
18: 1:
22:15
2: 15
6:15
20: 32
22:15
2:15
6: 15
16:15
6:15
18:15
2: 15
1C: 15
20:26
21:26
22:53
0:45
2:15
6: 15
4:15
1 x : ! 5
HRS
HRS
H.RS
HRS
HRS
MRS
hRS
HRS
HRS
_hRS
hRS
HRS
HRS
r.RS
HRS
HRS
HRS
"RS
HRS
HRS
HRS
hRS
« ?C:15 HRS
it
^l
4:15
4:15
12: 15
HRS
HRS
33.60
39. CO
42.00
47. CO
51. CO
A V E
41.30
42. CO
47. CO
51. CO
A V E
37. CO
51. CO
A V E
39. CO
47. CO
55. CO
A V E
41.20
42.20
42. 6C
45.50
47. CO
51. CO
A V E
25.00
3 3. CO
41. CO
49.00
T
HRS (ET)
H'SS (ET)
HRS JET)
KRS (ET)
HRS (ET!
RAGE:
.-HRS..!E!>
HRS (ET)
HRS (ET)
H.RS (ET)
RAGE:
HRS (ET)
hRS (ET)
RAGE:
HRS (ET)
HSS (ET!
hRS (ET)
RAGE:
HRS (ET)
HRS (ET)
HRS i£T)
HSS (ET)
HRS (ET)
HRS (ET)
RAGE:
HRS (ET)
HSS (ET)
HRS (ET)
HRS (ET)
0 T A L :
RATE:
25. CO HRS <£T)
33. CO
T
HRS (ET)
0 T A L :
S02 CCNC INLET- FLLE GAS
S02 CCNC INLET ?LUE Ct~
SC2 CCNC INLET FLUE G£S
S02 CCNC INLET FLLE GJS
S02 CCNC INLET FLUE GiS
S02 CCNC INLET FLUE G££
S02 CCNC CUTLET FLLE G ' i
S02 CCNC CUTLET FLUE CiC,
S02 CCNC CUTLET FLUE G.':i
S02 CCNC CUTLET FLUE G/-".
S02 CCKC CUTLET FLUE G.-,';
H20 CCNC INLET. FLUE G.!.'.
H20 CCNC INLET FLUE GAf,
h20 CCNC INLET FLUE GAS
CRIFICE PRESSURE ORCP
CRIFICE PRESSURE CROP
CRIFICE PRESSURE ORCP
CRIFICE PRESSURE ORCP
ORIFICE TEMPERATURE
CRIFICE TE'-'PERATLRE
CRIFICE TENP'JRATURc
ORIFICE TEt-'PERATLSE
ORIFICE TEMPERATURE
CRIFICE TEPFERATV.RE
CRIFICE TEr-'FERATLRH
HEIGHT CYCLCNE CLST
w = 'C-:-T CYCLCN; CUST
HEIGHT CYCLCNE CLST
HEIGHT CYCLCNE CLST
' WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DUST
HEIGHT CCLLECTCR DUST
WEIGHT CCLLECTCR DLST
U=IGHT CCLLECTCR DUST
WEIGHT CCLLECTCR DUST
-------
"i/21/74
12:15
2J.CC (-3S (tT)
4S.GO H=S iET)
TOT .'. L :
AVS
rt.S (fc'TL.
HftS..(ET>_
SAGc :
HEIGHT CARBCN
C-'?.2C.?-
TCT
TOT
S G\ CYCUCNE CLST
S CN CYCLCNE DL5T
iCV- 12)
CCV- 12!
JCV:- .12.
! C ii 12
t_ e- 11
J DT. ll
f D- 11
CH121T)
CW12!T!
/ _c 111, T } f_
/_ C11 i 1, T ! »_
/ AClli =
16: 15 H?.S
6:15 i-SS
27. CO !-. E ! G H T )
S (WEIGHT)
; (v.;i
NJ
H
f-
f.
-------
4/21/74
PAGE 3
C 1 A
C A R B C N
PRECCNDITICNER
21: 15
i 1:15
1 5:i5
21:15
1:15
: 5:15
' 4:15
:' 12:15
> 16:15
6:15
HRS
HRS
HRS
HRS
HRS
HRS
HRS
MRS
HRS
URS
42. CO
* f f\ "i
*» C U v
5C.CO
A V £
42.00
46.00
5C.CO
A V E
35. CO
3-.CO
T
37. CO
5 i . C 0
A V E
HRS
H.RS
P.
( ET t
I :
(ET!
(ET)
G E :
% TCT S CN INLET CAREC?>
s TOT s c:\ INLET CAREC?.
4 TCT S Cf. I ".'LET CAScCN
J! T3T S CN PJLET C
'. D-3jl)
i D-3C1)
/
1
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1
/
1
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1
1
t
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Z 3C 11 1 , T ) =
Z301 :i,T) =
Z301'.liT) =
A Z 30 1 i -
Z 20 1 t 2 1 T ) «
Z30i(2,T ! =
Z33i;2,T) =
AZ3012 =
COSOHTi =
C030KT) =
W0301 =
SD3CI =
D20i!ltT! =
C3Ci;i,T) =
AD 30 I i =
6.340
7.940
£.060
7 . 4 " 7
10.700
6.£OC
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10.167
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c.o
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20:15 HRS
1:15 HSS
S: 2 HRS
23:53 HRS
5:38 HP.S
20:15 HRS
l: 15 HRS
8: 2 HRS
23:50 HSS
5:38 r.RS
20:15 HRS
1:15 HRS
8: 2 HRS
44.60 HRS f=T)
5C,<-0 HSS (ET)
AVERAGE :
41.00 HSS (ET)
46.00 HSS iET)
c } Q ^ U~? ' C~*~ \
AVERAGE :
44.60 HSS !ET>
5C.40 HSS (ET)
AVERAGE:
41. CO HSS IET)
46. CO HRS JET)
52.30 HRS
52.30 HRS !ET)
AVERAGE:
SULFUR e
S02 CCNC CUTLET 'GAS
SQ2 CCNC CUTLET GAS
S02 CCNC CUTLET GiS
!-2S CCNC INLET GAS
H2S CCN'C. IMET GAS
r25 ~C"«C INLEI GAS
H2S CCNC INLET GAS
H2S CCNC CUTLET GAS
H-2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
HZ CCNC INLET GAS
i-2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
S-2 CCNC CUTLET GAS
H.2 CONC CUTLET GAS
r-2 CCNC CUTLET GAS
H20 CCNC INLET GAS
H20 CCNC INLET GAS
H20 CONC INLET GAS
H20 CCNC INLET GAS
H2C CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2Q CCKiC CUTLET GAS
N'2 CQNC INLET GAS
N2 CONC INLST GAS
M2 CCNC INLET GiS
N'2 CCNC INLET GAS
ENERATCR
1GS-206) /
{GS-2C61 /
. (GS-206! /
IGS-200) /
".GS-2C01 /
iff -jri n > /
' C; 5 £.\* V 1 f
, (GS-2CC! /
(GS-206! /
JGS-206) /
(GS-206) /
(GS-2CO! /
(GS-20C) /
(C-S-2CO! /
(GS-2CC) /
(GS-2C6) /
=
Y206(2,T) =
.AY206B =
Y200(3tT! =
Y2C:! 3-,~l =
AY200C =
Y206t3,T) *
Y2C6I3.T! =
AY20£C *
Y200(4,1 ) =
Y200(4,T) =
Y2CO(4,T) =
AY2CCD =
Y2C£C4,1 ) «
Y206(4,T; =
AY206C =
v>rnfc.Ti s
Y2CO(5,T) =
Y200(5»T5 =
AY200E =
4/21/74 PAGE 4
0.700 J (VOLUME)
0.990
C.S45
47.500
46.900
& 7 x t" *"*
47.200
7.500
5. 300
6.65C
~'"C.O ""
0.0
0.0
0.0
0.0
0.0
c.o
c.c
0.0
0.0
0.0
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49.SOO
48.900
52.500
53.100
52. SCO
52.50C
? (VCLUME)
\ (VCLUME)
? ( VCLUME)
% (VOLUME) :
0 ( vn UMF )
? (VOLUME)
7, (VCLUME)
3 (VCLUME) -5
S (VCLUMS)
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S (VCLUME!
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5:15 HRS
21:15 HRS
l:li HRS
5:15 HRS
21:15 HSS
5:15 HRS
44.60 HRS (ET)
5C.40 HRS (ET)
AVERAGE:
37.00 HRS (ET)
51. CO HRS iET)
AVERAGE:
45.00 HRS t£T)
46.00 HRS (ET)
5C.CO HRS (ET)
AVERAGE :
42. CO HRS (£T)
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AVERAGE:
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sc.co HRS ;ET>
N2 CCNC CUTLET GAS
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N2 OGNC CUTLET GAS
N2 INLET VCL FLOW RATS
N2 IN'LET VCL FLC* RATE
N2 INLET VCL FLCH RAT3
% TCT S ON IN'LET CARSCA
i TOT S CN INLET C*REC\
3 TOT S CN INLET CAS2:\
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t u->-> "\ r * ' T ': <~K
ff f£.w v^<> ltiw'^1 V,W>uv«l*
« H2Q CN IN'-;* CARBON
1GS-206) /
Y206(5,T) =
IGS-2C6! / Y206(;,T) =
(GS-206) / AY206E =
{ G-2CO) /
! G-20C! /
f G-2CC) /
(CS-3C2! /
(CS-302) /
(CS-3C2) /
ICS-302) /
(CS-200! /
ICE-2CC) /
(CS-2T.C! /
4CS-20C) /
ICS-JC2) /
"CCS-3C2) /
CCS-3C2) /
G200(5rT) =
G2CC(5,T) »
AG2COE =
Ji02(ltT) =
Z2C2I1.T1 =
Z302(1,T) «
AZ302A =
Z20C(1, T) =
Z2t5Ca,T) =
Z2CC!l,Ti =
A2200A =
Z3C2!2,T! =
Z302!2,T; =
43.800
43.400
43.6CO
106. COO
IC6.000
1C6.COO
6.340
7.940
8.060
7.447
6.040
22.900
22.6^0
17.193
10.700
6 . j C 0
13. COO
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CFH (70 CEG F) ,:
? (XEIGHT)
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v. 21:15 HRS 4?.SQ
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t£T)
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(ET)
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; H20 CN
% H20 CN
S H20 CN
% H2C CN
* AGIO CN
% ACIC CN
* iCIC ON
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INLET .-CARSCN
CUTLET CAR8CV
CUTLET C/SR6CS
CUTLET CAREC\
CUTLET. CARSC1*
CUTLET CARE:K
CUTLET C4REZN
C'JTLET CARE;^
CUTLET C*RE>
ICS-302)
JCS-2CC)
(CS-2CC)
ICS-2CC)
=
Z2CC!2iT) =
Z2CO(2,Ti »
AZ200E =
Z2C:(3,T) =
Z20C!3,T! =
Z200(3,T) »
AZ20CC -
10
<*/;
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3-700
1
1
2
0
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74 PAGE 5 ;
(V.EIGH.T) y
(v, EIGHTS
(WEIGHT)
(WEIGHT)
.
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f
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22:26
4:
14:
15
32
HRS
HRS
HRS
H 2
43.20 HRS !ST)
45. CO HRS !ST)
AVERAGE :
59.30 HRS (ET)
AVERAGE:
S GENERATCR/SU
H2 CCNC INLET GAS
H2 CC.NC INLET GAS
H2 CCNC INLET GAS
H2 CONC CUTLET GAS
H2 CONC CUTLET GAS
LFUR STRIPPER
=
(GS-1CG)
(GS-1CO)
IGS-1C8)
tGS-lCE)
/ Y100J3.T) =
/ AYIOOC -
/ Y103(3,T) =
/ AY108C =
4/21/74 PAGE 6
49.400 % (VCLUME)
4-9.500
49.450
0.0
0.0
I
3
J
(VCLUME)
(VCLUKE)
(VCLUME)
(VCLUME)
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32
32
32
15
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15
15
15
JLS
15
15
15
15
15
16:15
6:
HRS
HRS
HRS
HRS
J3.S
H?,S
HRS
H', S
HRS
HRS
hRS
HRS
HRS
HRS
HRS
HRS
HRS
15 H.RS
43.20 H'-.S (£T>
45. co :-s.s :ET;
AVERAGE :
55.30 HRS (ET1
AVERAGE:
55.30 HRS tET}
AVERAGE:
59.30 HRS l=T>
AVERAGE:
37.00 HRS (ET)
51. CO HRS !ET)
AVERAGE :
25.00 HRS 1ET)
33. CO HHS (ET!
41. CO HRS !ET!
49. CO HRS tET)
TOTAL:
RATE:
25.00 HRS (ET)
45. CO HRS (ET)
TOTAL:
RATE:
42. CO HRS 1ET)
46. CO HRS (cT)
5C.CO HRS (ET)
AVERAGE:
37.00 HRS IET).
51. CO HRS (ET!
AVERAGE :
N2 CD.NC INLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CCNC CUTLET GAS
N2 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2Q CCNC CUTLET GAS
H2C CCNC CUTLET GAS
N2 INLET VCL FLCV R*TE
N2 INLET VCL FLC* R4TE
?42 IMET VCL FLCV. RME
IsEIGHT CYCLC^r CUST
*EIGr7 CYCLCNc CcST
WEIGHT CYCLCNE OUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE CLST
VEIGHT CYCLCNE DUST
WEIGHT FILTER CUST
«EiGi-T FILTER CUST
isStGHT FILTER CLST
HEIGHT FILTER CUST
% TOT S CN CYCLONE OlST
Z TOT S CN CYCLONE OtST
S TOT S CN CYCLCHE CLST
% TDT S G,\ CYCLC.NE CLST
S TOT S CN FILTER DLT.T
% TOT S CN FILTER OLST
S TCT S C-N FILTER DLST
(GS-iCC
;GS-ICO
f GS-ICC
(Gs-ica
(cs-ioa
jGS-ica)
GS-1C8)
( G s i o a )
tcs-ica)
( G-1CO)
( C-JCC)
{ G-ICO;
! D-101!
! 0-101)
( 0-101)
r D-101!
( D-101)
( D-1C1)
f >* 7 rj j *
( C-iC-2 !
( C-1C2!
( D-102)
{ 0-lCl)
1 0-101)
C 0-1C1)
! C-1C1)
{ D-102)
( D-1C2)
t D-102)
/ Y1CO(;,T) =
/ YlQOiS.T! =
/ AY10CE =
/ Y108(5,T) =
/ AY106E =
/ AY1CSE -
/ Y108(4,7) =
/ AY103D =
/ G100(5,T>
/ G!CC(5,T! =
/ AGIQOE =
/ C010KT) =
/ CDlOliT ! =
/ CD 10 1(7) =
CD 10 1 ( T i =
/ wcici =
/ RD1C1 =
/ C01C2!7) =
/ CD1C21T) =
/ KCIC2 =
/ RD102 =
/ OlOHl.T) =
/ C1CK1.T) =
/ D10K1.T) =
/ ACL01A =
/ 0102(1, T) =
/ C1C2I1.T) =
/ A0102A =
5C.6CO
50.500
5C.550
55.200
55.200
35.000
35.000
7. £00
7.800
121.000
121. OCO
121.000
0.0
0.020
0.010
C.020
0.050
O.C02
0.0
0.0
0.0
0.0
2.720
3.200
3.640
3.137
0.0
0.0
0.0
&t s* w
%
S
S
?
%
?
I VCLUME)
(VCLUME)
(VCLU.XE)
(VCLUME)
(VCLUME)
(VCLUME)
(VCLUHE)
(VCLUME)
(VCLUHE)
't'
\3
!'i
!^
1
g
'.-s
-.
f.
^k
CFH (7C CEG F) W
CFH (7C CEG F) -,
CFH (70 OEG F) -
LB
Le
L3
L8
LE
LB
L3
IS
LE
LB
2
\
I
3
*
CUST
CUST
CUST
CUST
CUST
CUST/HR
CUST
CUST
CUST
CUST/hR
UEIGHT)
UEIGH.T)
I WEIGHT)
(V.SIGHT)
(HEIGHT)
IhEIGHT)
(HEIGHT)
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n
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34
3
3A
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a
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-------
W21/74
PAGE
00
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CARBCN I IV V
21:15 HRS A?. CO HRS tfT) ? RFMC^At > CM CARRf\
1--15 HRS 46.00 HRS (ET) % RESIDUAL S CN CARSC.N
5:15 HRS 5C.CO HRS (ET) % RESICUAL S CN CAR2CH
AVERAGE: * RESIDUAL S CN CARECf.
21:15 HRS 42. CO HRS (ET) % RESIDUAL H2C ON CARECiv
1:15 HRS 46. CO HRS (ET) % RESiCUSL H2C CN CARECA
5:15 HRS 5C.CO hRS ( ET ) ? RESIDUAL H2G CK CAREC^
AVERAGE: % RESIDUAL H2C CK CARGCIV
16:15 HRS 37. CO HRS (ET) CARBCN RECYCLE RATE
6:15 HRS 51.00 HRS (ET) CARBCN RECYCLE RATE
AVERAGE : CARBCN RECYCLE RATE
S U L F L R C C
Ifc:i5 HRS 37.00 HSS (ET) WEIGHT SULFUR CCLLEC1EC
6--15 KRS 51. CO HRS !ET) WEIGHT SULFUR COLLECTED
TOTAL: HEIGHT SULFUR COLLECTS
RATE: WEIGHT SULFUR COLLECUC
. .
ENTCRY HCPPER
!CS- 90) / Z90(1,T) =
.'CS- 50) / 290 (1-
-------
NJ
STATUS REPORT CF OPERATING CONDITIONS FOR
"i
3;
OPERATING PERIOD:
CAT=: 4/21/74 TIME CF RSCCRC
CATE: 4/22/74 TIXE C~ RBCCRC
: 16:15 HR
: 0: Q H!:
IJvTEGRA
5 TO
S TC
4/21/74 . PAGE 8
TED OPERATION OF S02 RECOVERY PRCCESS
24: 0 HRS
6:15 HSS
i
:
.
'.'
k.
PRCCESS ELAPSED TIKE CF PFRIH3:
START 37,
CC HRS
/ END 51. CO f-RS LENGTH OF PERIOD: 14.00 hRS
' SUMMARY GF INTEGRATED PRCCESS PERFORMANCE:
;.
1. S02 REfCVAL
PRSC2 =
97. 7S
% (ACTUAL) 90. C ? (GCAL)
.
i'
t!
"3
,-r
,J :.-
%
r
:A
!<
»
-?
2. r2S UTILIZATION
3. ACID CONVERSION ( TC SULFUR)
4. 1-2 UTILIZATION (TO H2S)
5. SULFL'R RECOVERY
6. (-2 UTILIZATION 4" UNIT
FVCS '
PHChS =
P«
PUH2 =
£2.94
{.3.99
fcO.76
C.C
c.c
ICO. CO
S (ACTUAL! 95.0 * (GCAL)
% (ACTUAL! 99.0 ? IGCAL)
Z (ACTUAL) 90. C \ (GCAL)
S (ACTUAL) 100.0 % (GCAL) Or SCRBEO SC2
? (ACTUAL) 25. C \ (GCAU) OF STRIPPED SULFUR
3
'-i
4
ri
>
-»
?
:1
S3 " r*
:sj
r*\
(J
f -
w
B
»
&5
1 1
ft
w
Li
P
t !
P
L
J
7. RESIDUAL SULFUR ON CARECN
8. CARBON RECYCLE RATE (DS!
S. ACID LCADING i.\LET CARECN 6" UNIT
1C. ."OISTURE CONTENT INLET CARSCN 6" UNIT
11. ACID LCACING INLET CARECN 8" UNIT
12'. H.OISTURE --CKTENT INLET CAR8CN 8" UNIT
13. TOTAL ACID CONVERTED 6" UNIT
14. SULFUR CONVERSION (TO K2S )
15. SULFUR CONDENSER EFFICIENCY
PAJCX EVENTS DURING OPERATING PERIOD:
BY-PASSED 18" UNIT OUST COLLECTOR
X90A =
RC90 =
X301C =
X3018 =
X302C =
X3028 »
PVC =
PSCI-S *
ERV400=
37.0 HRS.
C.C337
;<,32i
C. 2134
C.. 1411
C..2134
C.. 1411
S8.15
i;!C.63
C.O
LB S/LE C
L8 C(OE)/HR
LB ACIC/L3 C
L3 H2C/L3 C
LB ACIC/L9 C
LB H2C/LB C
it
%
%
'r,1
-t
-,
3J
"§
b^
t -
^
-".
j
*t
H
PLUS GAS STARTED 37.4 hRS. AT 3 FT/SEC.
CYLINDER I-2S TC £" UNIT STARTED 4C
.0 HRS.
L, H' TC 4" UNIT STARTED 40.6 HRS.; GAS VELOCITY
:'..G FT/ScU.
,,'
' S
CFF GAS 4"""LMT GCI.\G TO BURNER
-------
STATUS REPCP.T
f'; OPERATI'.G PtSTCC:
CATS: i/j.s/74
-
P.
..t
I ft
: INLET
: INLET
-
;i
C L- T
-. C-.TLET
i' CUTLET
GAS AS S02
c AS SESICL*L s
T C T A L IN:
GAS AS S02
CARSCN
V y CYCLCNE CUST
Vf y CCLLECTCR CUST
v-> « CARECN
=s T
H
2*
W I N
pi INLET
'35
W ' C U T .._..._
r, CUTLET
V.ESPAGE
C T A L CUT:
6" 0 I A C A
CA33CN
T C T A L IN:
CA33CN
ic CYCLC.NE CUST
=- T
1 '
k>
- i IN
L- INLET
U ' INLET
,^,
CUT
-. OL'TLE i
V CL'TLET
:- CUTLET
'.- T
C T A L CUT:
S U L
GAS AS H2S !CYL!
GAS AS r2S (PRCC)
T C T A_L I N :
GAS AS H2S
GAS AS SC2
CAS8CN
C T A L 0 U _T . :
s o 2 :
( G-
( C-
iRV-
! G-
/ r~
» V*
! C-
( C-
IC..-
(Rv-
R B 0 N
( C-
(RV-.
( C-
( C-.
(SV-
F U R
( G-
( G-
[ C-
!RV-
i : K B
13) /
11) /
1C) /
13! /
11) /
12) /
12) /
1C) /
P R E
12) /
:>co /
1! C 1 ) /
.1C I) /
:scc) /
GEN
iCl) /
2CC) /
? G-?C5) /
( G-2C5) /
I C-2C2! /
1P\-
2CC) /
E R
8G1CA =
BC11* =
SI 10 =
BCi3i =
3C12A =
BD11A =
B012/S =
BCW12A =
SO 10 =
CONDI
EC12A =
SI 300 =
8C201A =
60301A =
S0200 =
E R A T C R
6G2G1B =
6G203R =
3C2014 =
SI20C =
EC-2053 =
EG20SA =
8C202A =
S0200 =
2.
\s *
3.
0.
3.
A27£
9879
4157
0539
0312
C.01A6
0.
C
O.C051
3.
T I
3.
3.
3.
0.
3.
i .
C.
3.
10.
> ^
r\
6.
7.
10A7
C N E
C312
02 12
0312
0
0212
3554
C
C312
1703
26CA
7710
L3
LB
L£
LB
IS
LB
* n
LB
" *
R
L£
IS
LE
L6
IE'
LE
L£
L;
L;
L=
SDLFUR/HR
SULFUR/HR
SLLFUR/i-R
SLiLFUR/hR
SL.'LrUR/1-R
SCLFUR/hR
SULFUR/HR
S(JLFUR/I-R
SULFliR/HR
SULFUR/hR
SLLFUR/rR
SULFUR/I-R
SULFUR/HR
SULFUR/i-R
SULFUR/!-R
SULFUS/HR
SULFUR/t-R
StLFUS/hR
suLFUR/sa
SLLFUR/.-R
SULFUR/i-S
SL'LFUR/HR
1
.-
1
: i
'.4*
r
t
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;,
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-='
i!
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3=
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-.'
-.-
.3
a
^
-------
4/21/74
PAGE 10
OO
H 2 S G E \
ERATCR/SL
I N
INLET CAR30N
CUT
OUTLET
CUTLET
CUTLET
CYCLCNE
FILTEP
T
i M
TCTAL I
CAR3C\:
CAS AS h2S
GAS AS S
CUST
CUST
C T A L C U
0 V E R A
INLET GAS 18" UNIT AS
INLET GAS 3" UNIT AS
T C T
CUT
OUTLET
CYCLCNE
N :
-
T :
L L
SC2
CYL H2S
A L
GAS 18" UNIT AS SC2
CUST 13" UMT
COLLECTOR CUST 18" UMT
CAR2CN hEEPAGE 18" UMT
CYCLCNE CUST 6" UMT
CUTLET
OUTLET
CUTLET
GAS 8" UNIT AS
H2S
GAS 8" LN'IT AS SC2
GAS 4" UMT AS
OUTLET GAS 4" UNIT AS
CYCLCNS CUST 4" UNIT
FILTER CUST 4" UNIT
T C T A
H2S
S.
L S
{ C-2-:2)
(Rv-i :ci
I C-1C3)
( G-i:i)
( c-i:ii
i 0-1:21
tRv-i:ci
S U L F L
( G- 10:
( G-2C1:
S U L F L
< G- 13!
< D- 11!
( C- 12!
-------
4/21/74
PAGE 11
HYORCGEN MATERIAL
OO
N>
V
S U L F
*
UR CENERATC
R
!;]
IN . !.|
INLET
INLET
INLET
INLET
INLET
GAS AS
GAS AS
GAS'AS "
GAS AS
CAR3CN
T C T
H2
H2S
(RV-i:O 1
' 5G205C =
' BG20SH =
' EG205C =
' BC202H =
' H02CO =
L F U R
' 8G103C =
' BC2C2H =
' H100 =
' BG104C =
' 8G104H =
C
0
C
0
*
0
0837
6158
C860
0.7855
S T
C
0
C
0
0
RIP
"
A
4921
0860
5781
0
3974
' 3G104C = C.C886
hOlOO
0
"
4860
LS
LE
LB
L3
LE
P E
L6
~L8
LE
LE
LE
LS
LE
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
R
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
KYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
:->i
U
n
H
H
a
;j
-i
H
18
'~i
^
H
:s
J
-------
APPENDIX A-12-4
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-6 (51 - 66 hours)
283
-------
oo
4/22/74
STATUS REPORT OF OPERATING CONDITIONS F0:i INTEGRATED OPERATION OF SC2 RECOVERY PROCESS
PAGE
OPERATING PERIOD:
V
' _, pRre?*$ FI 4p<;=c Ti«f
-
i
;|
i;
'-
'
\-*
.«
(
1
.-!
:
.^
nl
r
'i
PROCESS VARIABLES
10:15 HRS
14:15 HRS
18:15 HRS
22:15
11:15
15:15
18:15
22:15
6:15
21:15
HRS
H.RS
HRS
hRS
HRS
HRS
HIS
55. CD HRS
59.00 HRS
63.00 HRS
67.00 HRS
A V E R 4
56.00 HRS
6C.OO HRS
63.00 HRS
67.00 HRS
A V E R A
51.03 HRS
66.00 HSS
A V E R A
OF PERIOD: STAST JX.CC HI
..
f.1- LS
S
S02 CCNC INLET FLUE G,1S
S02 CCNC INLET FLUE G.sS
S02 CCNC INLET FLUE <5i»S
S02 CONC CUTLET PLUS CIAS
SQ2 CONC CUTLET FLUE GAS
S02 CCNC CUTLET FLUE CAS
S02 CCNC CUTLET FLUS GAS
S02 CCNC CUTLET FLUE CAS
H20 CCNC INLET PLUS G >S
H20 CCNC INLET FLUE SAS
H20 CCNC INLET PLUS MS
B E R
(GS-
49.00 HRS
65.00 HRS
T 0 T A
RAT
49.00 H^S
57. CO rRS
c5.CC rRS
(ET)
(=T)
L :
E :
(ET)
<£T)
(?T)
WEIGHT COLLECTOR OUST
WEIGHT COLLECTOR DUST
WEIGrtT COLLECTOR DUST
WEIGHT COLLECTOR OUST
WEIGHT CflRfiCN WESPAGE
WEIGHT C*RSCN WEcPAGE
WSICHT CAftBCf; WCEHAGc
c
0-
0-
0-
(CV>-
(Cl>
?Ci.-
12)
12)
12)
12)
12)
12)
12!
/ C012JT) =
/ C012(T) =
/ K312 =
/ R012 =
/ CW 1 2 ( T ! =
/ CW 1 Z ( T )
/ Cr.'12(T) =
0.0
0.0
0.0
0.0
0.0
0.060
0.040
LB CUST
L2 CUST
L3 CUST
L3 CUST/HR
LB CUST
LS CUST
L3 OUST
_,*
3
3
ii
-M
.5
-------
f -
I
I
f'l 12H5 HRS 57.
;=: 20:15 HRS 65.
I'j A y
i'l
'.>' ' 6:15 hRS 51.
21:15 HRS 66.
I'j A V
JJ:
r«i
?:!
M
TOTAL:
RATE:
CO
CO
E
00
CO
E
H»S IET!
HRS (ET)
RAGE:
K»S (BIT
HSS (ET)
RAGE:
WEIGHT CtRBCN WEEPAG!
XEIGHT CAR9CN WEEPAG1
S TOT S
X TCT S
Z TOT S
S TCT S
S TOT S
* TCT S
CN CYCLCN6
CN CYCLCNE
Cl\ CYCLCNS
C' ST
Cl.ST
Ol.'ST
CN CCLLECTCR CL'.iT
C\ CCLLECTOR CLIiT
CN CCLLECTOR CLST
(CVi-
{ C-
t 0-
( 0-
{ D-
C 0-
; o-
12)
12 )
11 !
11!
li)
121"
12 )
12!
/ WCH12 =
/ RCW12 =
/ 011(1. T) =
/ Cll(l.T) =
/ &011A =
/ 012(1. T) =
/ 012!1,T) =
/ AR 1 7 &
4/22/74 PAGE 2 ]
0.100 LB CUST
0.006 L8 CUST/HR
S
6.080 %
6.800 %
6.440 %
C.O %
0.0 ?
0.0 %
(ViEIGHT)
(ViEIC-HT) j
(WEIGHT) =
'.
(WEIGHT) .
("EIGHT) .
(KEIGHT) jrf
-
,
:
:r'
K5
00
Ul
C:
-------
4/22/74
PAGE 3
6" 0 I A
CARBON
P R E C C N C I
1 C M E R
oo
L
;'
:-'
:
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)!
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52
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:«
c*
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3-
R.-,'
C*'
P"
i
g
U
!-=;
till S TCT
AVERAGE: 3 TOT
13:15 t-RS 5S.".C t-P5 SET) i H20
17:15 hRS Si.C: i-5S t=T) ? !-2C
21:15 !r WEIGI-T
20.-15 HRS 65. CC r-SS ! £7 '< KHIGS-I
TOTAL: X-£IC;-:T
T i T E : VvEICHT
6:15 "RS 51. CO >-SS !ET) S TOT
21:15 KRS 66. CO i-KS (ET) S TCT
AVERAGE: * TOT
*
s CN INLET C^RECN
S C\ 1NLST C-'TtC'
S C.N iMET CiS3C"
S CN INLET CiRDC":
S Ctv INLET CAS6C'-
CN INLET CASecN
CN l\LcT CAP.SCN
CN IM.ET CAK3CX
CYCLCNE DCST
CVCLCixE C'JST
CYCLC.NS OUST
CYCLIC DLST
S CN CYCLCNE OUST
S CN CYCLCN6 OUST
S CN CYCLONE ocsr
?CS-3CU /
;cs-3cij /
(CS-301) /
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H2 COiNC INLET GAS
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H2 CCNC CUTLET GAS
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H2 CONC INLET GAS
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PAGE 7
CARBON
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OPERATING PERIOD:
CATE: 4/22/74 TIKE OF RECC
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RC: £:15 It.
START 51 .
4/22/74 .PAGE 8
INTEGRATED OPERATION OF S02 RECOVERY PROCESS
S TO 21:15 KRS :'
CC_HRS
SUfKARY CF INTEGRATED PROCESS PERFORMANCE:
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4. h2 UT!L!ZAT!CM (TO H2S )
5. SUCFLS RSCCVERY
6. 1-2 UTILIZATION 4'-.tMT
7. RESIDUAL SUIFU» ON CARBCN
B. CARECN RECYCLE RATE (08)
«!. iCIO LC»;i'.t- :-;L>T CiRSON 6" UNIT
PRS02 =
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14. SULFLR CC.XVERSIC^ (TC K2S)
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4/22/74
STATUS REPORT CF OPERATING CONDITIONS FCR INTEGRATED OPERATION CF SC2 RECOVERY PROCESS
PAGE 9
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OPERATING PERIOD:
TATF: 4/22/74 TIME C? RECORD
PROCESS =LAPSEC TIME CF PFRtCC:
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BCili =
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SULFUR/rR
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CUTLET GiS AS S02
OUTLET CARBON
T CTAL CUT:
{ C--2 ;2) / EC202A =
(RV-2:c) / 50200 =
<;.60?S IS SULFUR/HR
10.9331 L2 SL.'
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CUTLET GAS AS h2S
CUTLET GAS AS S
FILTER CUST
TCTAL CUT:
OVERALL
T *t
INLET GAS 18" UNIT AS SC2
INLET GAS 8" UNIT AS CYL H2S
TOTAL
CUT
OUTLET GAS 18" UNIT AS SC2
CYCLCNE DUST 18" UMT
COLLECTOR CUST 18" UNIT
CiSECN SEEPAGE 18" UMT
CYCLCNE CUST 6" UMT
CUTLET GAS 3" UNIT AS H2S
OUTLET GAS 8" UNIT AS SC2
CUTLET GiS 4" UMT AS H2S
OUTLET GAS 4" UMT AS S
CVCLCN£ CUST 4" UNIT
FT! TCIi ** * i C ^ A II i V T T
TOTAL S
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(Ru-lCC)
S L 1 F U
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{ 3-1C4)
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i c-icn
i r i r 7 \
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L F U R
/ 2CH02A =
/ SHOO =
/ EC1C3A =
/ EGIO'S =
C JiCl fi =
/ ec:o2; =
/ SC1CO =
R SAL
/ EG10A =
/ 8G201B =
R IN:
/ EG13A =
/ B011A =
/ 8DI2A =
/ BCW12A =
/ RD301A =
/ EG20SH =
/ 3C-205* =
/ 3G10-i8 «
/ 3G1C4S =
/ 8D101A =
t arii<~. 5A
OUT:
STRIP
9.6073
9.6078
1.1873
6.3602
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c.o
1.1998
C. 180=
6.3602
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0-p
7.8398
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4/22/74 PAGE 10
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;
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SULFUR/hR
SULFUR /HR ;
S'JiFUR/HR .:
SULFUR/HR :
SULFUR/hR
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f
SULFUR/HR
SULFUR/hR -
SULFUR/t-S
.
SULFUR/hR :
SULFUR/I-R :
SULFUR/f-R :
SULFUR/I-R
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SULFUR/hfi ;
SULFUR/I-R i
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-------
PACE 11
HYDRCGES MATERIAL BALANCE:
ro
vo
1
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i
ft
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t
~.
si
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jj
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55
I N
INI FT
INLET
INLET
INLET
CUT
CUTLET
OUTLET
OUTLET
OUTLET
1
I N
INL5T
INLET
CUTLET
OUTLET
GAS AS
GAS AS
GAS AS
GAS AS
CAK3CM
T C T
GAS AS
GAS AS
GAS AS
CAR3CN
C T A
H 2 S
GAS AS
CASSCN
T C T
S U
H2
H2S (CYL)
H2S (PRCC)
ft L. IN
H2S
1-20
t OUT
GENE
H2
L F U' R
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( G-
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A L IN
GAS AS H2
GAS AS
GAS AS
H2S
I-2G
: (R\<-
; G-
( G-
( C-
.CC!
tC^t)
.C1>
1C4)
/ 8G203C =
/ EG2C3B =
/ bG203 =
/ 8G203C =
/ 6C20IF =
/ S-I2CO =
/ SG205C =
/ BG205H =
/ 3G205S =
/ BC2C2H =
/ (-02 CO =
L F U R
/ 3G1C3C »
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/ HI1CO =
/ BGlOiC =
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-------
APPENDIX A-12-5
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-7 (66 - 81 hours)
295
-------
4/22/7*
STATUS REPORT CF OPERATING CCNCITIONS FCR INTEGRATED OPERATION CF S02 RECOVERY PROCESS
PAGE 1
N>
v£>
I
/T~
I1:
i;'
!.!
] ....
!*-
J
1 _ _ .__
V
»'
'
CAT?.- 4/22/74 TIME CF RECCRC: 21:15 H:S TO 24: 0
CATE: 4/23/74 T
PROCESS ELAPSFC fr^'?
PROCESS VAR!A9i = «:
IV.E CF RECCRC: 0: 0 t-f:S TC 12:15
CF PERICC: START tl ..CC HRS / END
HRS
HRS
.
1
J
\
»
.-
61.CC HRS LENGTH CF PERIOD: 15.00 HRS
FCR OPERATING PERIOD:
' *>'
i*
d
J*l
;«
f'h
y
L-J
t»
H-
w
H
00
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22:15
2:15
6:15
10: 15
22:15
2:15
6:15
10:45
21: 15
12:15
2:15
10:15
18:15
22: 2
0:20
4:15
7:20
10:15
12:15
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
20:15 HRS
4: 15 HRS
12:15 HRS
67. CO HRS
71.03 VPS
75. CO HR3
75. CO H?.S
A V E R A
67. CO HRS
71. CO HRS
75. CO HRS
75.50 HRS
A V t R A
66. CO .-RS
81.00 HRS
A V E R A
71. CO HRS
7S.CO HRS
S7.CC HRS
A V E R A
66. bO HRS
69.10 HRS
73. CO HRS
76.10 HRS
79.CO HPS
81.00 HRS
A V E R A
65. CC HRS
73.00 HRS
81. CO HRS
T 0 T A
RAT
(ET)
(ET)
(ET)
(ET)
G E :
(ET)
(£T)
(ET)
(ET)
G E :
(cT)
(ET)
G E :
!ET>
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IET)
G E :
(ET)
(ET)
iET)
JET!
S
SC2 CCNSC INLET FLUE G,'!;
S02 CCNC INLET FLLE G.'S
S02 CCNC INLET FLUE GAS
S02 CONC CUTLET FLUE K IS
S02 CCNC CUTLET FLUE G.S3
SC2 CCNC CUTLET FLUE 0.!S
SC2 CCNC CUTLET FLUE >".!S
S02 CCNC CUTLET FLUE R,SS
H20 CCNC INLET FLUE G 55
H20 CCNC INLET FLUE G 5:5
H20 CCNC INLET FLUE G IS
ORIFICE PRESSURE DROP
CRIFICE PRESSURE DROP
ORIFICE PRESSURE CRCP
CRIFICE PRESSURE DRCP
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE OUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE CUST
B E R
4: 15
12:15
HRS
HRS
HRS
HRS
HRS
66.00 HRS
81. CC HRS
T 0 T A
RAT
65. CO H?S
73. CO HRS
SI. CO HRS
(ET)
(ET)
L :
E :
(tT)
<£T>
1ST)
WEIGHT CCLLECTCR DUST
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR DUST
WEIGHT CCLLECTCR DUS1
WEICHT C/SRFlCN V.££P4Gt
WEIGHT CARSCN HcSPAGF
WEIGHT CARBCN WEEPAGE
« D-
I D-
( C-
{ 0^
(CW-
(CW-
12)
12!
12!
12)
12)
12!
12)
/ CD12!T) =
/ CC12(T! =
/ WC 12 «
/ R012 =
/ CW12(T) "
1 Cwii'iT) »
/ CU1Z(T) =
0.0
0.0
0.0
0.0
0.0
G.C
o.cee
L8 CUST
L6 CUST
LB CUST
L8 CUST/HR
18 CUST
LE CUST
LB CU'ST
3
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:A
-»
-------
PAGE 2
1
''; 21:15
' 12:15
'
i. 4:15
12:15
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a i
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% TCT
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r c
S
S
S
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CN CYCLCNE OUST
CN CYCi-CN'E CLS1
CN CYCLCNE CtST
CK CCLLECTCR CIS"
ON CCLLECTCR CLST
CN CCLLECTCR CISV
ccx-
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=
=
s:
s
=
0.088
0.005
0.0
0.0
0.0
7.020
6.740
6.880
LB CUST j
LB CUST/HR 1
3 (HEIGHT) *.
S (hEIGHT) :
? (WEIGHT) :.
V
% (WEIGHT) ::
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-------
PAGE 3
6" 0 I A
CARBON
COND
ONED
NJ
VO
00
_l:15_H*_S_
5:15 i-'^S
9:15 H'.S
_5: 15 HRS
_9J-15_HR_SI
12:15 HRS
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12:15 HRS
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74.CO HRS (ET)
7^.CC i-.'S 1ET)
A V E R i. G j__:_
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A V E"R A G E :
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T_0_!_ A L' ;_
a A T E :
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A V E RAGEi
%_70T_S CN__INLET__CAREC:.
~% TCT S"CN INLET CiRiC.."
% TOT S CN tMET C^RtC .
z TCT s .cfv INLET CARFCA
~% 7^2 H20 CN INLET CAR3CN _
Z I-"2C CN INLET CiRBCK "
>?IC-rT CYCLCNE DLST_
J*E IGHT* CyCLCNE "CUST^
V.E IGr'T'CYCLCNE'CUST
S TOT S CN CYCLCNE DUST
t TCT S CK CYCLONE CU.'.T
Z TOT S CN CYCLCNE OUST
(CS-3C1)
5CS-3C1)
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f CS-301}
I , T ) =
Z3Cltl,T) -*
AZ3C14 =
Z30H2.T) =
Z301(2tT) =
AZ301E =
CD30KT) =
C0301 IT) =
VJ03C1 =
RD301 =
C301(1,T) »
D301U.T) =
AC301A *
8.880
S.S40
3.620
8.713
10.800
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16: 15 HRS
21:56 Has
2:56 HRS
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16:15 HRS
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2:56 HRS
6:45 hRS
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21:56 HRS
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6:45 HRS
21:15 HRS
12:15 HRS
1--15 HRS
5:15 HRS
9:15 HRS
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5:15 HRS
9:15 HRS
5:15 HRS
9: IS HRS
66.70 HRS (ET)
71.70 HRS tcT)
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AVERAGE:
69.70 HRS (ET)
85.00 HRS (ET)
AVERAGE :
56.70 HRS !ET)
71.70 HRS (ET)
75.50 HRS icT!
AVERAGE:
69. 7C HRS (ET)
85..CO H-S (=T)
V c R A u c :
66.70 HRS (£7!
71.70 HRS !ET)
AVERAGE:
69.70 HRS (ET)
6 5. CO HRS (ET)
AVERAGE:
66. 7D HRS (ET!
71.70 t-RS (ET)
75.50 HRS (ET)
AVERAGE :
69.70 HRS !£T)
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AVERAGE:
, t ~t f\ «'OC t ^"* \
66.70 rRS ( «: i )
71.70 HRS <=T)
75.50 HRS (ET)
AVERAGE:
66.00 HRS (ET)
81. CO HPS IET)
AVERAGE:
7C.CO HRS (ET)
74. CC HRS (ET)
73. CO HRS (ET)
AVERAGE:
7C.CO HRS (ET)
74. CO HSS (ETi
78. CO HRS " r* \
(GS-2C6)
SGS-2C6)
(GS-2C6)
(GS-2CO)
(GS-2CO)
JGS-2CO)
{GS-206!
(GS-206)
(C-S-2C6)
iGS-2C5>
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(GS-2CC!
(SS-2CC!
t f =
/ *G2COc »
/ Z302!1,T) =
/ Z302(1,T) =
/ Z302C.T) =
/ A23C2A =
/ Z2CO ! 1 e" ) «
/ Z2CC(1,T) -
/ AZ200A =
/ Z302I2,T> =
/ AZ3022 =
4/22/74 PAGE 4. j
1
1
0.950 J (VCLUME) J
1.210 3 (VCLUVE! iO
1.300 S (VCLL'KE) !:;
1.153 ? (VCLUKc) !=!
32.200 * (VCLUME) 1=1
27.200 ? (VCLUME! X
29.700 ? (VCLUME) -^
3.200 3 (VCLUME) i-i
0.700 S (VCLUME) -^
0.500 S (VCLUf.E) :i
1.467 S (VCLUME) >-j
0.0 S (VCLUHE) ''«'
0.0 ? (VCLUXE) -s
Of\ 5fV/f"IIIMPl
0.0 ? IVCLUME1 -i
0.0 ? (VCLUME)
0.0 I (VCLUf'E) »
14.000 I (VCLUfE) !=?'
21.200 « (VCLUME) r,'
17.600 J (VCLUME! :i
49.600 « (VCLUXE! -.'.
52.500 ? (VCLUME) *
52.9CO ? (VCLUME) T.
51.667 ? (VCLUMS) '-i
i>
53.300 ? (VCLUME) :,
51.100 S (VCLU.VE)
52.200 ? 1VCLUKE) -T
Z*
4*5 fif*O SfUPIIJMPl '-i
45.200 % (VCLUME) -^
45.000 S (VCLUME) '.-
45.333 J (VCLUME) ;.
121. COO CFH (70 CEG F) ..
121.000 CFH (7C CEG F)
121.000 CFH (7C OEC F) .,
S.8SO 3 (HEIGHT)
6.640 ?(» EIGHT) '...
S.620 S ("EIGHT)
8.713 i (WEIGHT! .
a
21.600 S (SEIGHT1
23.400 S (>.E:GH7!
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9.350 t (WEIGHT)
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74.
78.
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74.
78.
A V
CO
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CO
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HRS
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HRS
R A
HRS
HRS
R A
(ET)
IET)
!ET)
G E :
(ET)
(ET)
1ST)
G E :
% H20
% H20
% H2C
% ACID
% ACIC
% ACIC
ON
ON
CIS
HN
"CN
CUTLET CASECK
CUTLET CARECN
CUTLET CifEC
CUTLET
CUTLET
CA?.[
C
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(CS-2CO)
(CS-2CC)
(CS-20C)
(CS-2CO)
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«CS-2CO)
-------
4/22/74
PAGS
i'l
ij
t\
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1
22:56
13: 2
C: 8
4:56
0:38
22:56
13: 2
HRS
HRS
HRS
HRS
HRS
HRS
HRS
67.70
SI. SO
A V E
63.90
73.70
93.40
A V E
67. 7C
31.80
A V E
HRS
H*S
R A
HRS
HSS
HRS
R 1
HRS
HRS
R A
H 2
G E :
S GENERATOR'IU
H2 CCNC INLET G«S
H2 CCNC INLET GAS
H2 CCNC INLET CAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
LFUR STRIPPER
IGS-1CO) / Y100(3,T) =
(GS-1CC)
5GS-1CC!
JGS-108)
(GS-1CE!
ics-ioei
{GS-1CC!
;
S (VCLUNE) ;.,
3 (VCLUKE) !»
S IVCLUME) !.
S (VCLUKE) j'
S (VCLUKE) :-i
? (VCLUCE1 . -.,
s (VCLUKE) ;
1 '=?'
j
S
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0: 8
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14:35
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HRS
63.90
73.70
83. 4C
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HRS
HRS
HRS
R A
(ET;
1£T)
(ET)
G F. :
N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
N2 CQNC CUTLET GAS
(tT!
G £ :
(ET)
(ET)
G E :
(ET!
(ET!
(ET!
A L :
T E :
!£T)
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T E :
(ET!
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(ET)
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(£T>
t£T)
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2C CCNC CUTLET GAS
H2C CCNC CUTLET GAS
H2C CCNC CUTLET GAS
H20 CCNC CUTLET GAS
N2 INLET VCL FLOV, RATE
N2 INLET VCL FLC'« RATE
N2 INLET VCL FLCh RATE
HEIGHT CYCLCNE CLST
t-EIGrT CYCLCNE DUST
WEIGHT CYCLCNE DL'ST
ViEIGHT CYCLCNE CLST
HEIGHT CYCLCNE CL'ST
HEIGHT FILTER CLST
WEIGHT FILTER OUST
V.EIGHT rlLT;:' CUST
wcIGHT FILTER CLST
% TOT S CN CYCLONE CLST
% TOT S CN CYCLCNE CLST
% TOT S CN CYCLCNE OLST
% TOT S CN CYCLCNE DLST
S TDT S CN FILTER OLST
S TOT S CN FILTER OLST
S TCT S C;\ rIL~E* 3:.ST
{GS-106!
IGS-10E)
JGS-lOe)
(GS-103!
(GS-106!
IGS-103)
JGS-1CS)
(GS-108)
{ G-1CC)
{ G-1CC)
1 G-1CC)
( C-101)
; c-ici)
{ D-101)
( D-101)
( D-101)
t C-1C2)
! 0-1C?.)
( C-IC2S
! C-1C2!
j D-iOl)
{ D-101!
'. D-101 '
i C-iCl )
i C-102!
; c-102 )
; D-102)
/
/
-/
/
~i
/
'\
1
1
/
1
1
J.
1
/
/
/
',
Y1C8!2,T) =
Y108(2,T) =
Y1C8(2,T) =
AY10E2 =
Y103(4,T) =
Y1C8;4,T) =
AY108C *
6100(5, T) =
G1CO! 5,T ! =
AG100E =
CD10HT! =
C01CK7) =
C010KT) =
WD101 -=
P.01C1 =
CC102IT) =
C01'J2(T) =
1.0102 =
RD102 =
CICm.T) -
0101(1, T) =
D101 Jl.T)' =
ADI CIA =
Ci02(l,7) =
SIC«102* =
34.400
32.900
29.600
32.300
11.000
14.100
19.500
14.867
221.000
121. CCO
121. COO
0.0
0.0
0.0
0.0
0.0
0.0
. 0.0
0.0
0.0
» (VCLUME) '-.
J (VCLUHE) V
% (VCLU.ME) u
? (VCLUNE!
12
Z (VCLUHE) ii
S (VCLUf-e) y
S (VCLUME)
? (VCLUHE) U1
CFH (7C CEG F) -,
CFH (7C CEG F)
CFH (70 OEG F)
LB CUST i,
L8 CUST -3
LB CUST 3.'
LB CUST :j
LB CUST/HR
LE DUST
L5 CUST
LS CUST
L2 CUST/hR
,'
5.160 ? (fiEIGHT) -J
5.230 2 ('"EIGHT! J
^.")73>
0.0
0.0
0.0
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a (WEIGHT;
* («EICHT)
* (HEIGHT) .,
-------
PAGE
CA1BCN
INVENTORY
H C ? P E R
u>
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::
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5:15 H3S 74. CO HRS (£7) % P.ESICUAL S C,\ CARECx
9:15 FRS 78. CO H-JS (ET) S SESICUAL S CN CAS6C,\
AVERAGE: Z RESICUAL S CN CAR£C\
1:15 HRS 7C_no PBS l FT ) « RESIDUAL H.2C ON CAS3CN
5:15 HRS T^.CO HRS IET) S RESIDUAL H2C CN C«;CN
9:15 HRS 73. 1C K^S (ET) i R£S:£UAi. K2C CX CAR3CN
AVERAGE: S RESICUAL H2C CN CAR2CK
21:15 HRS 66. CO HRS IET) CARSON RECYCLE RATE
12:15 HRS 31.00 HRS (ET) CAR6CN RECYCLE RATE
AVERAGE: CARfiCN RECYCLE RATE
SULFUR C C N
20:15 HRS 65. CO HRS f ET ) V.E1GHT SULFUR COLLECTED
23:15 HRS 68. CO HRS IET) HEIGHT SULFUR CCLLECTEC
3:15 HRS 72. CO HRS (ET) WEIGHT SULFUR CClLcCT^C
7:15 HRS 76.00 HI^S (ET) V.ESCHT SULFUR CCLUCTEC
11:15 HSS 3C.CO H-i.S !ET) USICHT SULFUR CCLLECT:.C
TOTAL: KEIGH.T SULFUR COLLECT =c
SATE: *EIGHT SULFUR COLLECT =c
*
XS- 9C> / Z0(1.T ! =
CCS- 9C! / ZSO'.i.T; =
1CS- 90! / Z9CI1.7) =
(CS- 9C) / AZ9CA =
/ S«i(7) =
C S-'.C1) / SAOliT) =
s-4Ci : / s'.oitT > =
{ S-^01) / i«S«i31 =
! S- / RS'iOl =
5.160
5.2EO
3. S60
^.773
2.230
2.230
2.230
2.230
31.000
31.000
31.000
0.0
9.250
9.750
7.400
7.500
33.900
2. 260
? (WEIGHT)
I (V.EIGHT)
1 (WEIGHT)
S C«EIGKT)
I ! nEIGHT )
? (HEIGHT)
% (HEIGHT)
LB PAT'L/HR
L6 KAT'L/HR
LE KAT'L/HR
L8 SULFUR
L8 SULFUR
LB SULFUR
LB SULFUR
LE SULFUR
L2 SULFUR
LB SULFUR/HR
i
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~ 4/22/74
STiTUS REPORT CF OPERATING CONDITIONS FC^i I,\TEGRATED OPERATION OF S02 RECOVERY PROCESS
PAGE 8
o
CO
r"- CPERiTIN3P?RICO:
I.,
pi GATE: 4/22/74 TI*£ CF RECCRC
i'1 CAT = : 4/23/74 TIKE CF RECCRC
: 21:15 t
: 0: 0 :-
: i
RS TC 24: 0 HRS :
RS TC 12:1= HRS
PRCCESS £LA?SEC TIKE CF PERIOD:
START fce.CC HRS / END 61. CO >-RS LENGTH CF PERICD: 15.00 HRS
;: SUKXARY CF INTEGRATED PRCCESS PERFORMANCE:
ta
ft 1. SC2 REfCVAL
'",
H: 3. ACID CONVERSION ! 70 SULFUR)
?'
>>. 4. t-2 UTILIZATION ( TC H2S>
'-.i
! 5. SLLFLR RECOVERY
f;
3'.
» 6. ^ UTILIZATION 4" UMT
PRS02 =
PVCS =
PI-CHS »
FRS
FUH2 =
'i
.
96.29 3 (ACTUAL) 90.0 * (GCAL)
94.31 Z liCTUii.) 55. C S -:CCAL)
81.66 % (ACTUAL! 99. C ? (GCAL) -
\r
78.56 I (ACTUAL) 9C.C ? (GCAL)
-.
97. 4C -i (/.CTUAL) iCO.C S CC-CAL! OF SGS3HC SC2
33.20 % (ACTUAL: 25. c % (GOAD CF STRIPPED SULFUR
KO.CO %
pj ;i
tJ 7. RESIDUAL SULFUR CM CARECN
! t ' "" , , ...
F--
» 8. C»RBON RECYCLE RATE IDE)
p 9. ACID LCACISC- IMLET CARECN 6" UNIT
W 1C. COISTURE CONTENT INLET CARBCN 6" UNIT
p 11. ACID LOADING IMLET CARECSv 8" UNIT
t- 12. "OISTURr CONTENT INLET CARSCN 8" UNIT
ps
i. 13. TOTAL ACIC CCNVEPTEO £" UNIT
;.-: 14. SLLFUR CCNVC-SSICN ITO H2S1
i
15. SULFUR CONDENSER EFFICIENCY
X9CA -
RC90 =
X301C =
X3013 =
X202C »
X3028 =
FVC »
PSCI-S =
EP.V40C-
C.C513 L8 S/LE C ;«
26.329 LB C(DS!/HR :,
C.2158 LB ACIC/LB C :t
T
C.1307 L3 h2C/LS C ;,
C.2158 L3 ACIC/LB C -
C.1307 L3 h2C/L6 C =.
,,
91.85 *
9C.89 % -,
364.24 S .;
,.
!.-' J2
'-': CAJCR EVENTS DURING OPERATING PERICC:
« ' S'niTCHEO TC PRCCESS H2S AT 66.4.HRS._
L V.ITH INLET PRESSURE AT 46" TC 52"
H20
43
.S
VI
I- SULFUR CONDENSER *>AS CN STREAH CURING PERICi:
-------
4/22/74 PAGE
STATUS R=?C*T CF CPERATIN-G CCNCITICNS FCR INTEGRATES CPERATICS CF
PRCCESS ELAPSE
SULFUR V.ATFRIAI P.il 4K.
TIME" CF PERICD: STAR
CE (USING PROCESS H2S):
T " 46
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/ END '
-
SI. CO
HRS
LENGTH CF PERICC: 15.00 hRS
.
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£
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=:
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INLET
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S 0
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GAS AS SC2
CAR5CM
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GAS AS h2S (PRCC1
CA.'.ECN
TCTAL IN:
GAS AS F2S
GAS AE SC2
CAP3CN
C T A L OUT:
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SULFUR/1-R
SULFUR/HP.
SULFUR/hR
StLFUR/S-R
SULFU-R/!-R
SULFUR/1-R
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4/22/74
PAG= 10
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T f T f 1
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INLET GAS IS"
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UNIT AS
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COLLECTOR DUST
C*?.ECN 1.CEPAGE
CVCLCN? CUST 6
OUTLET GAS 8"
OUTLET GAS 8"
CUTLET GAS 4"
OUTLET GAS 4"
CYCLCNE CUST 4
FILTER CUST 4"
18" UMT
IS" UMT
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UNIT AS
UNIT AS
UNIT AS
UNIT AS
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UMT
T 0 T A
SC2
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( C-.-'C?) /
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( C- ' C 1 ) /
( c-:.c2) /
f o ti_ r r1 \ /
SULFUR
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( G-!C1) /
S U L FUR
( G- 13) /
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( G-1C4) /
( G-1C4) /
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t C-1C2) /
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BC103A
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-------
4/22/74
PAGE 11
HYDROGEN PATeaiAJ. BALANCE:
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OUTLET
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INLET
INLET
CUT
OUTLET
CUTLET
OUTLET
T
GAS
GAS"
S U L F
AS H2
AS H2S 1CYL)
GAS AS I-2S (PRCC) .
GAS AS 1-20
C4RBC.\
T r
GAS
GAS
GAS
T A L IN:
AS H2
AS H2S
AS H20
CA23CN
C T
H 2
GAS
A L OUT:
S GENERA
AS H2
CARBON
T C
GAS
GAS
GAS
C T
T A L IN:
AS H2
AS H2S
AS t-2Q
A L OUT:
U R GtNERATC
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t G- >C3) /
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( C !C3) 1
t C-.JC1) I
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i c-;?C2) >
(Rv-:?co i
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( G- 1C3) /
{ C-2C2) 1
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t G-IC^) /
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iRV-LCC) ;
' BG203C
' EG2C3B
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' 3G205C
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HYCRCCEN/HR
HYCRCGEN/hR
KYCRCGEN/hR
HYCRCGEM/HR
KYCF.CGtN/HS
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HYCRCGEM/i-R
HYCRCGEN/HR
R
HYCRCGEN/I-R
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-------
APPENDIX A-12-6
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-7 (81 - 96 hours)
307
-------
4/23/74
STATUS REPCRT CF OPERATING CCNCITICNS FCF INTEGRATED CPERATICN OF SC2 RECOVERY PROCESS
PAGE
o
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OPERATING P£R!CO:
CATE: 4/23/74
V
CATE: 4/24/74
TIME CF RF.CCRC:--. 12:15 i-?.!; T:
C 54: 0 HRS :'
TIME CF RECCRC: 0: 0 HRS TO 3:15
PRCCESS SLAP'SFC Tl'fF CF PFRTCD: START- PI .rr na<; / FKT
PRrcs.ss v:aiiP'p<; PTR PPI
15: S
18:15
22:15
2:15
15:20
18:15
22:15
0:32
2:15
12:15
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HSS
3:15 HRS
18:15
2:15
14:32
16:26
19:15
21:20
l: 15
3:15
12:15
20:15
4: 15
12:15
12; 15
2C:15
4:15
HRS
HRS
HRS
hRS
HSS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HSS
H3S
HRS
HRS
33.90 HRS
67. CO HRS
91.00 HRS
95. CO HRS
A V E R A
84.10 HRS
67.00 HRS
91. CO HRS
93.30 HRS
95.00 HRS
(ET!
(ET)
(ET)
(ET1
G E :
(ET)
JIETJ_
(ET)
(ET)
(£T)
AVERAGE:
_81.CO_HRS_IEIJ
96.00 HRS (ET)
A V E R A
67.00 HRS
95. CO HRS
A V £ R A
83.20 HRS
65.20 HRS
S3. CD hRS
9C.10 HSS
94. CD H?.S
96. CO HRS
A V E R A
31.00 HRS
8S. CO HRS
97. CO HRS_
T 0 T A
RAT
31.00 HRS
97.00 HRS
T 3 T A
RAT
SI. CO hi»S
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(ET)
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(ET)
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(ET)
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S 0 2 SCR
S02 CCNC INLET FLLE G.'S
S02 CCNC INLET FLLE Gi S
S02 CCNC INLET FLUE G/S
S02 CCNC INLET FLLE G< S
SC2 CCNC INLET FLUE G/S
S02 CCNC CUTLET FLL'E i. AS
SC2 CCNC CUTLET FLLE CAS
SC2 CCNC CUTLET FLUE CAS
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4/23/74
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IS: 15 HRS 87. CC HRS (ETI WEIGHT SULFUR CCLLECTE!'
TOTAL: WEIGHT SULFUR CCLLECTE;:
RATE: WEIGHT SULFUR CCLLECTEi:
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PRCCESS cLAPSEC TIfE CF PERIOD
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: f
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SUMMARY CF INTEGRATED PRCCESS PERFORMANCE: . >!
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9. ACIO LCACING INLET CtRECK S" UNIT
10. H01STURE CCNTEttT l^aET CARSCN 6" UNIT
11. ACID LCACING IMLET CARBON S" UMT
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-------
4/23/74
STATUS R5?CRT CF CPERATING CCNCITICNS FCR 1MEGRATEO OPERATIC* CF S02 RECOVERY PROCESS
PAGE 9
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INLET
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CUTLET
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TIME OF RECCRC: 12:15 HRS TO 24: 0 s~
S
TIKE CF RECCRC: 0: 0 SfS TO 3:15 HSS
Tiy= CF PERIOD:
CE (USING PROCESS
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T C T A L IN
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PAGE 10
H 2 S
G £ N E R & T CR/SULFUR
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4/23/74
PAGE 11
HYQRCGEN MATERIAL Bi
u>
I-1
oo
IN.
TKIPT
T OL' f C T
INLET
I\LET
INLET
CUT
CUTLET
OUTLET
OUTLET
OUTLET
T
GAS AS.
r c * c
G.'.S AS
GAS AS
CAR3CN
T C T
GAS AS
GAS AS
GAS AS
CARBCIM
C T A
SDL
H2
iJ 5 C f f" VI \
r2S (PRCC)
H20
A L IN:
r2
H2S
L OUT:
FUR G = N
( G-2C3) /
!
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HYCRCGEN/I-R '.|
hYCRCGEN/HR '.
HYCRCGEN/hR H,
HYCP.CGEM/HR <;
HYCRCGSN/hR »'
HYCRCGEN/HR 1:-
lj
I N
INLET
INLET
1
I
i CUT
H 2 S
GAS AS
CASSCN
T C T
1 CUTLET GAS AS
! CUTLET
.OUTLET
! T
GAS AS
GAS AS
C T A
G E N E R
H2
A L IN:
H2
I-2S
H20
L GUT:
ATCS/SUL
! G-K3) /
( C-2C2) /
(Rv-lfC) /
( G-1C4) /
! G-114) /
! G-H4J /
(RV-:tCi /
FUR
BG103C =
EC202H =
HUGO =
BG104C =
SGlO'ii-i =
eGI04C =
K0100 -
S T R
0.
C.
0.
0.
C.
C.
0.
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4921
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-------
APPENDIX A-12-7
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-7 (96 - 111 hours)
319
-------
4/24/74
PAGE
CO
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O
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1 !
i.
4
STATUS REPCRT CF
OPERATING FERICO:
riTF: «/24/74
OPERATING CCNCITICMS FCP INTEGRATED CPERATICN CF S02
TIKE CF RECCRD: 3:15 t R«: TC 18:15
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HRS
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PAGE 7
C A F, 3 C N
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-------
PAGE
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STATUS RSPGRT OF OPERATING CCNCITICNS fC-: INTEGRATED OPERATION Cf S02 RECCVE3Y PROCESS
OPERATING PERICC:
D AT .£_: 4 / 2 A/ 74
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PROCESS ELAPSEC TIME OF PERIOD:
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L'ENGTH OF~~PER7CC: 15.00 HRS
CF INTEGRATED PRCC5SS ?ERFCR.VA,NCE:
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3. ACID CCNV = RS!Cr. ITO SULFUR) PVCS = 73.22 % {ACTUAL)
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STATUS REPORT CF OPERATING CONDITION'S FCR HT!:CRATEO OPERATION CF SC2 RECOVERY PROCESS
OPERATING PES.'OC:
CVTE: 4/2W7* TICS CF RECORD: 3:
.
PROCESS ELAPSED TIME CF PERIOD: START
SLLFLS NiT£RI«L 31LANCE (USING PROCESS P2S1:
S 0 2
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INLET GAS AS SC2
::;L=T c AS RESIDUAL S
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CUT
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CUTLET CARBCN
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INLET GAS AS H2S tPRCC)
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OUT
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LEIVGTH Or PERICD: 15-CO HRS
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PAGE 10
(jO
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PAGE 11
NYORCGEN ViTERIAL BALANCE:
SULFL'R GENERATOR
J *
INLET G/,S AS H2 t G-2C':0 / 3G203C"= _ 0.0 "" lie HY
_!NLET_GiS AS h2S_'! / BC2033 ^_I_0.0 12 KYCRCGEM/i-R '
i'.LET GAS AS H2S:?*CC> ('3-2C:.V/ 2-203 "= C. 3'i'lf IS" V.YCRCG £',/HS"
:N'.HT GAS AS 1-20 f C 2C2:l / EG2C3D = G.:-A51 IS HYCRCGEN/rR
_:.'i:.S_T_Ci.*3C'; ( C-2C;. ;_/__6C201 h__f C.!05*_L2 rYCRCGEN/KR_
T C T A L I N : (RV-2CC) / Ht2CO = 0.9917 LE~HYCRCG'EN/rR
CUT
CLTfHT Gi.S AS '^2 I 5-2 ;.!; / EG2:05C = 0,C L8'HYCRCGcN/HR
C^'lH-T GtS AS K2S ( G-ICt'> / a02C:.H = C.O Lc HfCRCGEN/f-.R
IpL_7lT" C~:iSC'. ('~C-'2ci:7"/"BC202V~= ~C.'l24J"CS~HYi:SCSEN/hS~
" "T"C f &~L OUT: ~(RV-2C"«:T /" 1-02CO = 0.3145 '\E~HYCRCC
H 2 S ' G S K E R A T 0 R ,' J. U L I- i; R' STRIP
IN _
:'.l£T CIS AS_H2 ' (_G-li;i)_ /_BG103C_= 0.4521 12 HYCaCO£N/!-R
" " "lr;L£LlCA=5CN _____ T C-2 :;;"! ^/_SC202H = '(
T C T A L IN: (P.V-!."!:! / hllOC = 3.6162
C L1 T . __ . .
_0-.'TLiT_GAS_>S_H2___ f. .G-lI'fl._/_SGsC4C = 0-0 L5
_OL-T!_rT GiS_iS_H2S , t_G1-.' 5_-/_sGi04H * O.J411 L5
"ctTLET C*S AS _r20 i~G-l :'")"/ 6G10'iC~= 'C.2'22l''_£
T"L T A L "b'JT: (RV- ICCi / hQICC' = 0.5632 L3
-------
APPENDIX A-12-8
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-7 (111 - 126 hours)
331
-------
PAGE 1
STAr'jS 3EPCRT CF OPERATING CCiNCITICNS FCR INVEGSATEO CPERiTICM CF SC2 RECOVERY PROCESS
OPERATING PERIOC:
- CATE: 4/24/7*
CAT E:
_II£E_C_F _RECCRCJ 18:_15_HRS_ TC 24: 0_HRS .
_TI.UE CF RECCRC: 0: 0 HRS TC 9:15 rRS
PS CC EC S . E L i?SEC _T_L'H_CF__P:R_!_CD_: _ST A Rj___1 _1_1_..0 C H RS / EN5_'126.CC HRS
LENGTH CF PERiCD: 15.00 HRS
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AVERAGE:
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20:15 HRS 113. CO H<*S «ET )
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_12:i5_hRS 129.CO HSSJET)
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4/24/74
PAGE 3
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,
.
ICS-2CC) / 2200(1. T) =
CS-2CC) / Z2COI1.T) =
(CS-iCO) / AZ200A =
(CS-302) / 2i:2!2-T! =
(CS-3C2I / Z2C2(2TTi =
JCS-3C2) / Z3C2(2,T) =
(CS-3C2) / AZ3C28 =
CCS-2CC) / Z200(2,T) =
ICS-2CC) / Z20C'.2,T) =
(CS-2CO) / Z2CC(2.T) =
SCS-2CC) / Z200'.2fT! =
JCS-2CC) / AZ20CE =
(CS-2CO) / Z200(3,T) =
(CS-2CC) / Z200O.T) =
(CS-2CO) / Z20C(3,T) =
ICS-2CC) / Z2CC(3,T) =
ICS-2CO) / AZ200C =
-
4/24/74 PAGE 5
19.640 5 (WEIGHT)
19.960 ? (WEIGHT)
19.640 % (WEIGHT)
5.900 ? (WEIGHT)
&.900 J (WEIGHT)
7.900 1 (WEIGHT)
9.100 ? (WEIGHT)
7.450 % (WEIGHT)
2.900 I (WEIGHT)
2.400 S (WEIGHT)
2.800 S (WEIGHT)
3.200 ? (WEIGHT)
2.825 S (WEIGHT)
3.040 S (WEIGHT)
2.400 * (WEIGHT)
2.350 * (WEIGHT)
2.450 ? (WEIGHT)
2.560 S (WEIGHT)
I
i
J
it
'',<
'.'
!;!
-.1
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T-I
J
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1
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4/24/74
PAGE
H 2 S
N E R A TOR /
tJL F U R
STRIPPER
U>
u>
l: 2 HRS
21:15 HPS
4:45 HRS
6:15 HftS
23: 2 HRS
3:50 HRS
9:26 HRS
1: 2 HRS
21: 15 HRS
4:45 HRS
6:15 HRS
23: 2 HRS
3:50 HRS
9:26 HSS
6:15 KRS
23: 2 HRS
3:50 HRS
9:26 HRS
6:15 HRS
23: 2 HRS
3:50 HRS
9:26 HRS
18:15 HRS
9:15 HRS
20:15 HRS
4:15 HRS
20:15 HRS .
4:15 HRS
21:15 HRS
1:15 HRS
5: 15 HRS
9:15 HRS
18:15 HRS
115 HRS
93.80 HSS
121.00 HSS (=T)
TOTAL:
RATE:
114. CO HRS (ET)
113. CO HRS !ET!
122. CO HSS !ET)
176. CO H5S !£T)
AVERAGE:
11 '..CO HRS tET)
** *?# 0 "} ^ ^ ^ ' ^ ~ )
A V ERASE:
(-2 CCNC INLET CAS
H2 CCNC IKLET GAS
H2 CCNC SKLET GAS
HZ CC\C INLET GAS
K2 CCNC CUTLET GAS
H2 CONC CUTLET GAS
H2 CONC CUTLET GAS
>2 CCMC CUTLET GAS
H2 CCNC CUTLET GAS
N2 CCKC INLET GAS
N2 CCKC INLET GAS
M2 CCKC INLST GAS
N2 CCNC INLET GAS
N2 CCNC CUTLET GAS
N2 CONC CUTLET GAS
S'2 CCNC CUTLET GAS
N2 CGN'C CUTLET GAS
M2 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H20 CCN'C CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H2Q CCN'C CUTLET GAS
i-20 CCNC CUTLET GAS
N2 IN-LET VCL FLOW RATE
N2 INLET VCL FLOS* RATE
N2 INLET VCL FLOW RATE
HEIGHT CYCLCNE DLST
hEIC-HT CYCLCNE CUST
HEIGHT CYCLCNE CUST
WEIGHT CYCLCNE OLST
WEIGHT FILTER CLST
WEIGHT FILTER CUST
fcrlGHT FILTER CUST
. W?!GHT FILTER OUST
% TOT S CN CYCLONE DUST
% TOT S CN CYCLCNE CLST
S 7DT S CN CYCLONE OUST
% TCT S CN CYCLCNE CtST
% TOT S CN CYCLCNE CLST
S TOT S CN FILTER OUST
* TCT S CN F'LTcR DL-S't
% TOT S CN FILTER CLST
(GS-1CO) / Y100(3,T) =
tGS-ICO) / Y1CC!3,T) =
1GS-1CO) / Y100(3,T) =
(GS-1CC) / AY1CCC =
«GS-108) / Y10B!3,T) «
IGS-iOS) / Y108t3,7> =
/ Y10S(4,T) =
JGS-106) / Y1C6(4,T> =
{GS-1C8J / Y1C6<4TT) =
JGS-103) / Y10S(4,T) =
5GS-108I / AYiCSO =
( G-1CC) / G10CI5.1) =
t G-1CO! / G100(5,T) =
I G-100) / AG10CE =
< D-101 / C010KT! =
(0-101 / CD10KT) =
( C-1C1 / «0101 =
( C-101 / ftClOl =
« D-102 / C0102(T! =
( D-102 / CD1C2IT) =
( C-1C2 / v;ci02 =
? D-102 / RC102 =
( 0-1C1) / ClCl(lfT) -
! 0-101; / 0101(1, T) =
? D-lCi; / CiOiEltTi »
( D-1C1) / CICKi.T) =
1 D-1C1 ) / A0101A =
( 0-102) / CIO 2! 1,7) =
i 0-1C2 1 / C.102 i ,7 ) =
{ 0-1C2) / AC102; =
50.600 t (VCLUKE)
51. COO J (VCLUME)
50.700 3 ! VCLUKE)
50.767 * (VCCUKE)
. 0.0 1 (VCLUME)
0.0 ? ( VCLUKE)
0.0 % (VCLU"=)
0.0 5 (VCLUME)
0.0 S ( VCLUME)
49.400 % ( VCLUME)
49.000 S (VCLUME)
49.300 J (VCLUME)
49.233 S (VCLUME)
52.200 ? (VCLU.XE!
52.200 S (VCL'JXE)
52.603 3 (VCLUME!
52. iOO % iVCLUMt!
52.425 S (VCLUME)
29.900 S t VCLUKE)
27.700 * (VCLUME!
26.300 3 (VCLUMJ)
26.500 Z (VCLUKE)
27.725 S (VCLUME)
17.600 ? (VCLUME)
19.700 % (VCLUME)
20.200 ? (VCLUME)
20.600 ? I VCLUME)
19.525 3 I VCLUKE)
1Z1.C03 CFK (7C CEG F)
121.000 CrH (7C CEG F)
121.000 CFH (7C DEC F)
0.0 LB CUST
O.COS LB CUST
O.C06 L6 CUST
O.C01 LB CUST/HR
0.0 LE CUST
0.0 LB CUST
C.O LB CUST
0.0 LS CUST/HR
2.440 3 (HEIGHT)
4.CCC 3 (HEIGHT)
'..640 ? ('.EirtHTl
3.960 ? !V. = 'GH7)
4.010 ? (SEIGHT)
0.0 S (UEIGHT)
0.0 5 l'*-IGrT)
0.0 J (WEIGHT)
"
^
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f
;-;
-»
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PAGE
CARBON
INVENTORY
HOPPER
U>
CO
71:
1:
5:
9:
21:
1:
5:
9:
15
H<*S
114. CO
15 hRS 118. :0
15 HRS 12J.CO
1.5 hRS 126, CO
15
15
15
15
HRS
HRS
HRS
.HRS
A V E
" 114. CO
US. CO
12Z.CC
126. CO
A V E
HSS
HSS
H3S
R A
HPS
H5S
HSS
"R A
(ET)
I=T>
(ET)
J ET 1
G E :
(ET)
(ET)
!ET)
1ST)
G E :
^ RESIDUAL S ON CARBCN
S RESIDUAL S CH CAR3CN
s RESIDUAL s CM CARECN
t RESIDUAL S CN CA38CN
t RESIDUAL S CM CARBCN
% RESIDUAL H2C
S RESIDUAL H2C
t RESIDUAL H2C
* RESIDUAL H2C
% RESIDUAL H20
CM CARECN
CN'CASSCN
ON CAR6CN
ON CARECN
ON CARECN
?CS- 9C) /
T (WEIGHT) [i
I (WEIGHT) \'
- I,
! (WEIGHT) 1.
? C«EIGHT)
? (ViEIGHT) '
* ('.EIGHT) j.
S (WEIGHT) t>
iij
18:
9:
15
1.5
HRS
HRS
111.00
126. CO
A V E
HRS
HRS
R i
IET)
G E :
CARECN RECYCLE
CAP8CN RECYCLE
CAR3GN RECYCLE
RATE
RATE
RATE
1 C- 90) /
J C- 901 /
1 C- 901 /
C901I.T) =
C90(1,T> =
31.000
31.000
31. COO
L8 KAT'L/HR M
LB. PiT'L/HR --i
LE ^AT'L/HR ft
T«
S U L
FUR C C N
DENSER
;?
'-^
22:
2:
6:
15
15
15
10:15
HRS
HRS
HRS
HRS
115.00
119. CO
123. GO
127.00
T
HRS
HSS
HSS
"HRS
0 T
R A
(ET)
(£T)
IET)
A L :
T E :
WEIGHT SULFUR
WEIGHT SULFUR
WHTGH.T SULFU3
HEIGHT SULFUR
WEIGHT SULFUR
WEIGHT SULFUR
COLLECTEC
COLLECTEC
CCLLECTEC
CCLLECTEE
CCLLECTEC
CCLLECTEC
S-401) /
S-401) /
S-401) /
S-401) /
S-401) /
S-401) /
S40KT) =
S401IT) »
S40K7) =
S40HT) =
. HS401 =
RS401 =
0.0
7.000
6.750
7.200
21.050
1.754
LB SULFUR j..
LB SULFUR *,
L6 SULFUR j,
LB SULFUR ij
L8 SULFUR ;V
L3 SULFUR/HR ~4
"*
a
sJ
-------
CO
Co
vo
f
I
4
* \
v
STATUS REPORT CF OPERATING CONDITIONS FC!
f'| OPERATING PERIOD:
>>'. CAT*: 4/24/74 TIME CF RPCCR£: 18:1? :
«'.
is!"
V
6
ni
\>L
CATE: 4/25/74 TIHE-DF RECCRC: 0: C :
PROCESS ELAPSED TIKE CF PERICO:
v
4/24/74 PiCE 8 '
: INTEGRATED OPERATION CF SC2 RECCVERY PROCESS i
i
RS TC.
rRS TC
START lli.CC WRS
24
0 HRS
-.
9:15 HRS
END" 126.00 VRS LENGTH CF PERICO: 15.00 hRS
.
,
SUCVARY GF INTEGRATED PROCESS PERFGRKAMIE:
1.
S02 RSPQVAL
FRS02 >
55. 3C
2
(ACTUAL) SO.C I (C-CAL)
-
?» - . -r
K
W
ft
N
s
w
2.
3.
4.
5.
6.
h2S UTP IZATICN
AC 1.0 CCXVERSICN (TO SULFUR)
H2 UTILIZftTICN (TO HZS )
SU.FLR RECOVERY
h2 UTILIZATION 4" UNIT
FVCS -
PH.CHS -
FRS '«=
FUH2 "
?9.B5
72.73
67.36
' 79.01
27.93
ICC. 00
X
2
X
?S.C % (GCAL)
JACTUiL) 50. C t CGCSLJ
,
(ACTUAL) 1CC.C * IGCAL) OF SGRBEC SC2
(AC'UAL) 25.0 S C GCAL ) OF STRIPPED SULFUR
" »
,
,
23
;.
bj rj
y
*--
tr
y
Q
£
L
1 ! '
35
H '
c:-
i ;
y-.
U
P
LJ
k-
U
7.
8.
RESIDUAL SULFUR ON CARBON
CASSCS RECYCLE RATE (CE)
9. ACIO LOADING INLET CiREC.N 6" UNIT
10.
11.
12.
13.
14.
15.
MOISTURE CONTENT IMLET CAR2CN 6" UNIT
ACIC LCACI.NG INLET CARSCti 8" UNIT
KBISTURE CONTENT INLET CARBCN 8" UNIT
TOTAL ACIC CONVERTED 6" UNIT
SULFLR CCM/ESSICS -TO HZS)
SULFUR CONDENSES EFFICIENCY
KAJOR EVENTS DURING OPERATING PERIOD:
PILCT PL^NT PLJCEC ON STAKC3Y AT
129.6 !-RS. TC CORRECT CARBON FE'EC
AT STG 6 CF THE 4" UNIT.
X90A »
RC90 »
X301C *
X301B "
X302C -
X302B -~
PVC
PSCI-S '
ERV400-
PR03LEM
C.C42S
2S.C44
C.2159
C.1C13
C.2I59
C.1C.13
84.36
£4.45
179.64
LB
LB
L3
LS
LB
LS
t
%
%
S/LE C
C!CB)/KS
ACiC/LB C
1-20/LE C
ACIC/L3 C
1-20/L8 C
I*
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;,
X
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2^
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it
STATUS REPORT CF OPERATING CCNCITIONS FCft INTEGRATED OPERATION CF SC2
OPERATING PERIOD:
CAT": 4/24/7* TIME C?"*£CCSC:
CATS: W2S/7* TIKE CF RCCCRC:
PRCCESS ELAPSED TIME CF PERICD:
18:15 !JSS
0: 0 HRS
START 111. CC
TC 24: 0 HSS
TC 9:15 KRS
HRS / END 126. CC fcRS
'i/2'./7<. PAGE
RECOVERY PROCESS
9
,
;
LENGTH CF PcRICC: 15.00 HRS .,
SCLFUR K4TESI«U BALANCE (USING PRCCESS -H2S) :
! N
INLET GAS 4S S02
INLET C AS RES10U«L S
T C T A L IN:
CUT
OUTLET GAS AS SC2
OUTLET .CARBCN
CYCLCNE CUST
COLLECTOR OUST
C*RECh SEEPAGE
TCTAL OUT:
6" D 1 A C A
S 0 2 S C
( 6-' 13)
< C-- 11)
IRV-- 10)
I 6- 13)
1 C- 12)
C C- il)
t D- 12 >
CCfc- 12)
1RV- 1C)
R B 0 N P
R B E R
/ SGlOi =
/ BC11A =
/ SI10 =
/ BGI3A =
/ 3C12A =
/ SOU A *
1 8012A '
1 ECW12A =
/ SOIC =
R E C 0 N D I T
2.3257
1.2431
3.572E
0.1095
3.29C3
0.0133
O.C
O.CC04
3.^135
I C N
LE
LB
LB
LE
L3
LS
LS
LB
L6
E R
S'JLFUR/hR
SULFUR/HR
SULFUR/:-R
SULFUR/HR
SL'LFUR/l-R
SULFtS/l-R
SULFUR/FR
SULFUR/HR
SULFUR/HR
T
= 3
1
('<
(J
--
"I
V
t<
^
_'
L, ~ _,'
* IN - =
P
to
^
PS
i
S*
a*
t '
to
r'
- " '
'**
1 ; '
5 -
j..
Lr
Ui
U
-
INLET CARSON
TCTAL IN:
CUT
OUTLET CARBON
CYCLCKE GUST
TCTAL OUT:
S U L
I N
ISLET GAS AS H2S (CYL)
INLET GAS AS S2S (PRCC)
INLET CARSON
TCTAL IN:
CUT
CUTLET GAS AS H2S
OUTLET GAS AS SC2
CUTLET CARBON
TCTAL OUT:
( C- 12)
1RV-3CC)
< C-2C1)
< C-301)
IRV-3CC)
FUR G E
1 G--2C1)
( G-2C1)
! C-2C1)
UV-2CC)
( G-2C5)
( G-3C5)
( C-2C2I
(U--2CO
/ BC12A =
/ SI300 =
/ EC 201* =
/ 80301A =
/ S0300 =
N E R A T C R
/ BG201S =
/ 3C203R =
/ BC201A =
/ SI200 =
/ 3G2055 =
/ 8G205A =
/ 8C202A =
/ S02CO =
3.2903
3.2903
3.2903
0.0
3.2903
0.0
5.2043
3.29C3
8.5952
O.C070
C.2491
7.7806
LE
LS
LE
LB
LS
LB
L8
LE
r- r- r*
m to n>
LE
SULFUR/HR
SL'LFUR/HR
SULFUR/HR
SULFUR/KR
SULFUR/HR
SULFUR /HR
SULF'JR/HR
SULFUR/hR
SULFUR /HR
SCLFUR/HR
SULFUR/HR
SULFUR/HR
-S
23
y
>
!o
U
U1
:'l
/U
-s
*,
:-'
H
fi
-------
4/24/74
PAGE 10
fi
H
-4
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'.1
7;
?'
H
i,,
p
e
K
W
H
H
ij
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B
U
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is
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H
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u
H
34.
i .
i .
L
P
P=
U
i!".
L
i
H2S GENERA!
IN-
INLET CARBCN . -
T C T A L IN:
CUT
OUTLET CARBON
CUTLET GAS AS H2S
OUTLET GAS AS S
CYCLCNE CUST
FILTER CUST
TCTAL OUTt
OVERALL
I N
INLET GAS 18" UNIT AS SC2
INLST GAS B" UNIT AS CYL H2S
TOTAL
CUT
OUTLET GAS 18" LSIT AS S02
CYCLCf^E CUST 18" UNIT
COLLECTOR DUST IS" UffIT
CARBCN WEEPAGE 18" UNIT
CYCLCNE DUST 6" L'.NIT
CUTLET GAS 8" LNIT AS_H2S.._.
OUTLET GAS 3" UNIT AS SC2
CUTLET GAS 4" UNIT AS H2S
CUTLET GAS 4" U.'ilT AS S
CYCLCNE CUST 4" LMT
FILTER CUST 4" U.NIT
TOTAL S
r o R / s u i
i C--2C2) /
MRV-1CC) /
«
C--1C3) /
G--1C4) /
G- 1C4) /
D- 1C1) /
C-1C2) /
(RV-1CC) /
S L '. F U R
( G- 1C) /
( G--2C1) /
S U . F U R
J G- 13) /
Q- 11) /
3- 12) /
CVr- 12) /
0--3C1) /
G-2C5) /
3-:2C5.) /
G--IC4) /
G-1C4! /
C-iCl) /
C-1C2) /
U L r- U R
-
.FUR
8C202* =
SHOO =
BC103« =
BC-104B =
BG104S =
B010LA =
S0102A =
S0100 =
B A L J
8G10A =
EG 20 IE =
I N :
BG13A =
BD11A =
ECK12A =
E03C1* =
BG2053 =
8G205* =
EG104E =
3G1C4S =
BD101* =
60102* =
OUT:
STRIPPER
7.5244 L8 SULFUR/H.R
7.5244 LB SULFUR/HR
1.2431 LS SULFUR/HR
5.2248 LB SULFUR/HR
1.7542 Lfi SULFUR/HR
C.QOOO LE SULFUR/HR
C.O LB SULFUR/HR
8.2022 LB SULFUR/HR
> K C E
2.3297 LB SULFUR/HR
C.O L8 SULFUR/HR
2.2297 13 SULFUS/HR
0.1C95 LH SULFUR/HR
0.0133 LB SULFUR/HR
0.0 LB SULFUR/HR
O.C004 LB SULFUR/HR
O.C LB SULFUR/HR
O.C070 LE SL'LFUR/HR
C.2491 LS SULFUR/H.R
C.O LS SULFUR/HR
i.7542 L2 SULFUS/HR
G.CCCC L3 SULFUR/KR
C.O LB SL'LFUR/HR
2.1335 LS SULFUR/HR
_
1
y
: i
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i
i (
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4
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. 1
«!
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jj
^
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'ci
f!.
-,
^
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-fc
'"*
Us
1
.;
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+f
J
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PAGc 11
U>
i
j HYC3CGEN MATERIAL BALANCE:
i
!'
Is1
:
i'!
»»
i
\*'
H
a
r
r"1
»-
y
73
v<
t-i
y
w --
Cd
P'1
I N
IMLET
INiLET
I?iL£T
INLET
: u T
OLTLcT
CUTLET
CUTLET
DLTLET
T
I N
s u
GAS AS H2
GAS AS H2S JCYL)
C-iS iS H2S (PRCC)
GiS AS H2C
CAP3CX
TOTAL IN
GAS AS H2
GAS AS K2S
GAS AS H20
CAR3C.N
C T A L CUT
H 2 S GENE
INLET GAS AS H2
INLET
CUT
OUTLET
OUTLET
OUTLET
T
CASSON
T C T A L IN
GAS AS H2
GAS AS H2S
GAS AS H20
C T A 1 OUT
L.f U R C E
.
t G-2C3J
( G-2(31
( C 2C3)
! C 2C3)
: m ru
LE
LS
LS
LS
P
"L8
LE
LE
LB
LS
IB
LE
j
' \
\
KYCRCGEN/HR
HYCRCGEN/HR -:
HYCRCGEN/rR
HYCRCGEN/HR t.
.1
HYCRCGEN/HR .>
KYCRCGEN/H-R -<
HYCRCC-E.V/HR ..;
KYCRCGEH/HR »?
'.»
E R W
i_'
HYCRCGEN/HR al
HYCRCGEN/HR i.;
HYCRCGEN/HR '-,'
HYCRCGEN/HR '-j
HYERCGEM/HR ~i
HYCRCGSX/I-R k.
HYCRCGEN/HR ;,J
^ 3S
-3
5-i S-'
BS
3-
1 ,
,
ZS
^
-'
U -=
M
-------
APPENDIX A-12-9
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-8 (144 - 148 hours)
343
-------
PAGE 1
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3. 300 ! (KEIGHT)
3.860 2 UcICHT)
3.830 t IWcIGrT)
2.100 % (WEIGHT)
2.900 J (HEIGHT)
1.700 1 (SicIGHT)
2.233 S (HEIGHT)
31.000 LB MAT'L/HR
31.000 LB PAT'L/KR
31.000 LB yAT*L/HR
0.0 L6 SULFUR
6.500 LE S'JLFUS
6.50C LB SULFUR
1.625 LE SULFUR/HR
-
'
;
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1 *
*-
STATUS RC-PCRT CF OPERATING CCNCITICNS
OPERATING PERIOD:
CATE: .4/26/74 TIf'E OF RECCRC: 3:1
.... PRCCESS Ft APSFT TK«F T.F PrRICC*:
START
4/26/74 PAGE 7
FCR INTEGRATED OPERATION OF 502 RECOVERY PROCESS
< rsS TC 7:15 KSS
1'4.CC HRS / END 148. CO »-RS LENGTH CF PERIOD: 4.00 HRS
* . ,
.1
i'"
SLMXiRY CF INTEGRATED PROCESS PERFORMANCE: ' =
1. SC2 RSfCVAL
PSS02
* 95.23 s (ACTUAL: 9c.o * (GCAD
.«'
-
-
^
a
2. V2S UT I LI I iT !C:j
3. ACID CC:.VE-3IC\ I TC S'JL.-UR)
4. H2 LTILIZATICN (TO H2S)
5. SULFUR RECOVERY
6. t-2 UTILI:;.T;C:; 4" US:T
7. RESIDUAL SULFUR ON CARBON
PUf-2S
?ucs
PHCHS
pas
PUH2
X90A
99.85 S {ACTUAL) 95. C 3 (GCAL)
77.23 % (' CTU.'-!.) 9.C S iGCAL)
70.70 % {ACTUAL) 90. C ? IGCAL)
72. 8£ % JACTUi!.; iCO.O * (CCAL) CF SCR3EC SC2
23.36 ''. !ACTU»L) 25. C S (GCAL) Of STRIFP6C SULrLR
= ICC. CO 3 :
.
C.C4C6 L8 S/LE C -
=",' :
"'
'..
fu
f
;-t
'-.
,;
P
y
0
;-:
uj
S. CARSON RECYCLE RATE !D3)
9. ACi~ LCiCi:\G li^Sl C*R2C:\ 6" UNIT
1C. MOISTURE_CCNTENT INLET CAR8CN 6" UNIT
11. 6CIO LCACING INLET CiRECN 8" UNIT
12. ."OISTURE CCNTENT IN-LET CARBON S" UNIT
' 13. TOTiL ACIC CCNV5RTED 8" UNIT
14. SULFUR CONVERSION (TO H2S)
15. SULFUR CCN'CENSER EFFICIENCY
PAJCR EVENTS DURING CFERATING PERICC:
CURING STANC6Y LEAK AT ORIFICE IN
PRTCESS !-2S LINE FCUNC AND REPAIR
EEFCRE RE-START UP.
CORRECTED SCALE OFFSET ON 4" UNIT
fcNJCP fEANT PREVIOUS 106 CFh SET
RC90
X301C
X3C18
X302C
X3C2E
PVC
PSCI-S
ERV40C
ED
N2 RCT;
FT.~"GAVF
29.120 LS C!DE)/HR
~'*~ia*.J_^4_\3>-'^#Lb-/tei~'W
C.C956 L3 H2C/LB C :
-
C.2294 LB ACiC/LS C
C.0956 LB S-2C/LS C ;
-
9C.29 S
= 8C.C3 % -
116.97 % .
__
,
'
.
fi:TER
KG CFH ACTUAL.
-------
9!
U1
1
i;i
!.;
V
!«.
:,l
STATUS REPCST CF OPERATING CCiVCITIONS
CPESATIfvO PERIOD:
CATE: 4/2*774 TIKE CF RECCRC: 3:
_
PRCCESS SLiPSEC TIME CP PERIOD: START
SULFUR MATERIAL BALANCE (USING PRCCESS H2S):
4/26/7^ PAGE 6
FtR INTEGRATED OPERATICN CF S02 RECCVERY PROCESS
15 hlS
1 4.CC
TC 7:15 HRS
HRS / END 148.
:
.
CO hRS LENGTH CF PEfUCD: A. 00 hRS :
t
i
i
r- : : -:
r
r~
K__
h' -
S 0 2
: N
INLET GAS AS £02
INLET C AS RESIDLAL S
TCTAL IN:
; c
! :- 13)
< r- ID
tRs- 1C)
R 3 E R
/ 3G10A =
/ ECU* =
/ sno =
2.3A02 LB SULFUR/hR
1.1873 13 SULFUR/hR
3.5275 LS SULFUR/hR
~!~ C U 7
s
zt
y
B*1*"
_
-..
w
1 1
u
y
**!
k*
v.
S
CUTLET S.'.S AS SCE
C'-TLET Ci?3C\
CYC' C^5 DUST
CDLL5CTCS OUST
CARBCN KEEPAGE
TOTAL OUT:
6" 0 I i _C A__B S C
I N
INLET CAS8CN
TCTAL IKS
CUT
OUTLET CAR3CN
CYCLCNE DUST
TCTAL OUT:
S U L F C
; :- is;
( f- 12:
( f- 12)
(C'.- 121
(RV- 1C)
!> P
I C- 12)
(?V-3CC!
( C-2C1)
i r-sci)
(F.V-3CCI
R G E
1 BC12A =
/ ED12A =
.' 8CK'12* =
/ SD1C =
S E C G N ~ I T
/ 8C124 =
/ SI3CO =
/ SC20H =
/ BD3CI4 =
/ S03DO =
X E R A T C R
C.1IC4 IS SLLF'JS/HR
3.365C LS SULFUR/HR
C-v LE SLiLFUS/hR r
O.C091 LB SULFUR/hR r
3.5075 LB S'JLFUR/hR -
: c N E s -
_
-
3.3688 L3 SULFUR/hR -
3.3638 LS SULFUR/HR ' ;
3.3683 LS SULFUS/1-S
0.0 LB SULFUR/HR
3.3688 LE SULFUR/HR ..
-
U
L-L
:.j
P '
^:
. _ .. .
r--
I N
INLET GAS AS h2S (CYL)
INLET GAS AS H2S tPROC)
INLET CARSON
TOTAL IN':
CUT
OUTLET GAS AS h2S
CUTLET GAS AS S02
CUTLET CAS8CN
TCTAL CUT:
{ 0-2C1)
1 1.-2C1)
( C-2C1)
t-!"-ZCC)
{ G-2C5)
( G-2C5)
t C-2C2)
1 t'--2CC)
/ BC2013 =
/ BG2C3R =
/ 3C201* =
/ SI2CO =
/ 3C205E =
/ S02CO =
0.0 LE SULFUR/hR
5.5679 LE SULFUR/t-a
3.3638 LE SULFU^/HR
3. 9367 16 SULFUr/hR
_
C.C07A LE SULFUR/i-R
3.2615 LB SULFCR/hn
8.1A44 L2 SULFL.R/HR
6.4133 L3 SULFUR/i-R
I?
a .... ...... . ... .
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f
i
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.i'
'i
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f'
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'7
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fc
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, -.
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.
H2S GEKERA
I N
INLET CAR^C?C
TOTAL IN: '
CUT
CUTLET CARBON
CUTLET GAS AS H2S
CUTLET C-AS AS S
CYCLCNE CUST
?ILT£R CUST
TCTAL CUT:
OVERALL
t N
INLET GAS IS" UNIT AS SC2
INLET GAS 8" UNIT AS CVL H2S
TOTAL
CUT
CUTLET GAS 18" UNIT AS SC2
CYCLCI\E CUST 18" L'NIT
COLLECTOR CUST 16" UMT
CARSCN V.EEPAGE IS" UNIT
CYCLCNE C'JST 6" LMT
CUTLET GiS 8" UMT AS H2S
OUTLET GAS 8« UNIT AS sc2
CUTLET GAS A" UNIT AS H2S
CUTLET GAS 4" UNIT AS S
CYCLCNt CUST 4" UNIT
FKTER CUST 4" LMT
TCTAL S
TOR/ S U L
t C-2C2) /
(RV -ICC) . /
1 C-1C3) /
( G-1C4) /
r G-lCn) /
( C-iCI) /
( C-IC2) /
(R'i--lCC) /
S L .FUR
( C 1C) /
( C 2C1) /
S '- . ? U R
( C 131 /
i t- 11 > /
{ r- 12} /
(CV- 12) /
( [ -3C1! /
t C-2C5) /
i C- C5) /
( G- C4) /
( (.- C4) /
< L'-- Cl) /
'. t:-!C2) /
U L r U ft
,
F L R
SC2026
SI1CC
SC103A
3G104B
EG10R
SUS.FUR/i-3
SULFUR/t-R
S^,L^l.'i^/^?.
SULFUR/1-R
SULFUR/l-R
SULFUR/HR
SULFUR/I-R
SULFUR/l-S
SULFUR/hR
SULFUR/hR
SULFUR/rR
SULFUR/HR
S'.LFL'R/l-a
SULFUR/i-R
SULFUR/i-R .
SCLFUR/rR
SULFUR/hR
SULFUR/HR .
SULFUR/t-R
\
'.
.
-
. -
"1
j,
'-,
«
72
-t
:4
-'
r.
3,
Zl
^
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-
-T
f-
a
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.-
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t
1 HYD*CG£N MATERIAL BALANCE:
> S U L F
»3_ _
'; IN
= ' iNLET GAS AS H2
INLET GAS AS 1-2S (CYL)
'"' INLET GAS AS H2S (PRCC) -
I'' INLET GAS AS H2C
':: IN' £T CARSON
-.-. T C T A L I N :
:;i
;r CUT
?* OUTLET GAS AS H2
\i. OUTLET GAS AS H2S
p OUTLET GAS AS >-2C
'. OUTLET CAR3CN
TCTALOUT:
\\
t'-.
'- H2S GENERA
U IN
p INLET GAS AS H2
'si INLET CARBON
U.
~ - CUT
-.-. CUTLET GAS AS H2
i. CUTLET GAS AS H2S
to1 CUTLET GAS AS 1-20
e-- TCTALOUT:
r I
S-.
;s
'fc:
U
f=
L; R G E
t (,-:>C3)
( c-;:c3)
( c;-;!C3)
( G-,!C3>
( >;jci)
{RV-:!CC>
I C-;!C5)
< G-.2C5)
( :-.?c2)
T 0 =. / S U
< G-IC3)
( C-JC2)
CRV-1CC)
< C-1C4)
J G-1C4)
1 C-1C4)
iP'-lCC)
N E R A T C R
/ BG203C =
/ 8G203B =
/ BG203 =
/ 8G203D =
/ BC201H =
/ *I200 =
/ SG205C -
/ EG205H =
/ EG205C =
/ BC202H =
/ H3200 =
L F t R S
/ BG103C =
/ BC202H »
/ HIiOO =
/ BG104C «
/ BG104H =
/ SG1040 =
/ i-OICO =
4/26/74 PAGE 10
0.0 LE HYCRCGEN/1-R
O.C LE HYCRCGEf
-------
APPENDIX A-12-10
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-8 (148 - 156 hours)
354
-------
OJ
Ui
Ci
4/26/74
STATUS REPORT Cr OPERATING CONDITIONS F:!R INTEGRATED OPERATION CF SC2 RECOVERY PROCESS
PAGE
I
!«:
OPERATING PERIOD:
CiTE: 4/26/74
TTJ'5 OF RSCCRC: 7:15 HRS
TO 15:15 HRS
':
.
: PROCESS ELi?S=C TtVE OF PERIM: START K.S.CC HRS / END 156. CO HRS LENGTH CF PERIOD: 8.00 HRS ;.
ft .
jti
PROCESS
',
VARIABLES PCS OPERATING PERICC: . !
fi . >
i'= SC2SC-RBER
'**;
P
W
»
L,'
10:26 «tS
14:26 HRS
13:15 HRS
10:45 hRS
14:32 HRS
IS: 15 H.RS
151.20 HRS (ET)
155.20 HRS (ET)
159. CO HRS (ET)
AVERAGE:
151.50 HRS (£T)
155.30 HRS (ET!
159. CO HRS !ET)
AVERAGE:
S02 CC.NC INLET FLUE 'iS
S02 CCNC INLET FLUE i..*S
S02 CCNC I.NLET FLUE 3*3
S02 CCNC INLET FLU'E 5*S
S02 CONC CUTLET FLUE GJS
SC2 CCNC CUTLET FLUE GiS
502 CC.NC CUTLET FLUE GJS
S02 CCNC CUTLET FLUE CAS
(GS- 1C) /
tGS- 1C) /
(GS- 10) /
tGS- 1C) /
!GS- 16) /
TOTAL:
SATE:
(-20 CONC INLET FLUE 0-KS (sTJ
161. CO K-S ;£Ti
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR CUST
WEIGHT CiRSCN WEEPiCE
WSIGH.T C/..-.ECN V.SEPiCE
V.EICKT CiRSCN '.vEEPtCE
WEIGHT CARECN W'ErP;C =
* TCT S CN CYCLONE CUiiT
S TCT S C.N CYCLCNS CUI-T
I TCT S C.S CYCLCKE CU5.T
( 0- 12) /
1 D- 12) /
5 D- 12! /
< C- 12) /
!CW- 12) /
:cv.- 12: /
«.Cl.- 12) /
-------
f»
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I ;
h«
-------
Ul
_I51.CO. .KS
4 V S S
6" OIA CARBON
?_JCT__S_.CN_ INL.ET
: S TCT S CN I'.'LET
_1C:15 Has 151.CO HRS 1ST)
_.1«:15 HRS 155.CO I-^S (6T>
_1S_:15 HRS 153.00
2C:15
7:15 HRS
15:15 hR5_
A V E S A G 6 :
__153.-0 !-.s!S..!cTi__
161.00 J-RSjl£TJ
" T_C T_Ali_:
R"A T £ ;
148.CO rSS (ET!
A~~ v" 'E~T'~A~G' e'T"
i H2o"oN"i\LEt"CARBON"
S H20 CN INLET CARBCN
V h20~CV INLET ""
_V.ZIGHT CYCLC.'JE DUST
J»EJGHT_CYCLCKE CUST_J__
_hEIGKT CYCLCN'E'DUST ' '
ME IGh77~C'Y'Cl"CN£ DUST "
s TOT s C.N CYCLCKE CLSV
_S_T07_S C^_C^CLCNS_OLS"
X TO'r S~CN CVCLCNE DUST"
4/26/7* PAGc 3
PRSCONCITICNER
iCS-iCl) / Z3GU1,7) = 9.080 3 (WEIGHT)
iCS-30;! / Z3CI;l,TS = 9.niO ? ttiEIGH.T)
(CS-3C1) / AliOIi » 9.470 ? (kEIG^T)
(CS-3C1) / Z3CH2.T! = 7.000 S («£IGt-T)
ICS-3C1) / i3CH2,T) = 7.000 Z (UEIGHi)
{CS-3~1) / £331(2. T) = 5.603 S (V.EIGHT)
(CS-3C1) / AJ301E = 6.533 5 !V.£;GI-T)
{ D-3CI5 / CD301iT: = 0.0 L3 CUST
S D-301) / CD3:i:T! » 0.0 LS CUST
I D-30U / K3301 = 0-0 LS CL'ST
( C-3C1J / RD3C1 = C.O LS CbST/hR
r C-3C'n / DSOltltT) = C.O S thEJGhT!
S 3-3CI) / CSQUl.t) = C.O % {hilGhTJ
1 C-301) / AD30Li = 0.0 S IhEIC-HT)
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SULFUR
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13:32 HRS
.. 14:56 HRS
13:32 HRS
., 14:56 HRS
13:32 HRS
14:5fc HRS
13:32 HRS
14:56 HRS
13:32 HRS
7:15 HRS
15:15 HRS
1C: 15 H~S
14: 15 HRS
10:15 HRS
14:15 HRS
13:15 HSS
10:15 HRS
14: 15 HRS
18:15 HRS
10:15 HRS
14:15 HRS
18:15 HRS
10: 15 HRS
14:15 HRS
IS: 15 HRS
154.30
A v E
155.70
V e
" 154.30
A V E
15.5*70
A V E
154.30
A V E
155.70
A V 6
154.30
A V t
155.70.
A V =
154.30
A V E
IAS. 00
156. CO
A V E
155.00
i V E
151. CO
155. GO
159. jO
151. CO
155.00
15?. CO
A V £
151-00
155. CO
159. CO
A V £
151. DO
155. CO
159.00
A V E
HRS 1ST)
RAGE:
HRS !ET)
AGE:
HRS
HSS ;ET; . .
rRS (ET)
RAGE:
S02 CCNC CUTLET GAS
S02 CCNC CUTLET GiS
H2S CCNC INLET GAS
H2S CCi>C INLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET C-iS
H2 CGNC INLET GAS
H2 CCNC INLET GAS
H2 CGNC CUTLET GAS
H2 CCN'C CUTLET GAS
H20 CC.NC INLET GAS
H20 CONC INLET GAS
H20 CONC CUTLET GAS
H20 CCriC CUTLET GiS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CONC CUTLET GAS
N2 CCNC OUTLET GAS
M2 IN'.ET VCL FLO* RA" =
N2 INLET VCL FLC'rf RATE
N2 INLET VCL FLGH RJ"E
Z TGT S CN INLET OSKSCN
s: TOT s CN I::LET C^P-::CN
X TOT S CN INLET CiRHCN
? TOT S CN- CUTLET C^=, tC\
% TOT S CN CUTLET CJI'.cCv
S TCr S Ci\ CUTLET C^-.£C<
% TCT S C.\ CUTLET C^KEC>
% H20 CN INLET CARBCIi
% H2C ON INLET CARSC:.
S H20 CN INLET CARSC.\
% H20 CN INLET C.1RBC.-;
S H2u CN CUT'.cT CAR2CI
? H20 CN CUTLET C*R3::r
S J-20 ON CUTLET CARB^
? H2C ON CUTLET CAR3'^
S ACID ON' CUTLET CA3:LN
? AC!D CN CUTLET C*' :CN
* ACIC CN CUTLET CA?3llN
% ACIC ON CUTLET CARKN
(G?-2C6)
iGS-2Ci!
!GS-20C)
(GS-2CO)
SGS-2C6)
1C-S-206)
{6S-2C01
JGS-2CC)
(GS-2C6)
(GS-2CO)
(GS-2CC)
tGS-206 )
(VCLUHE)
(VCLU«E)
(VCLUHE)
(VCLUME)
FK !7C CEG F)
:
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1
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n
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CFH !7C CEG r)
CFH (7C CEG F) -
i
9
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s
?
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! WEIGHT)
(V.EIGHT)
!WcIGHT)
(HEIGHT)
("EIGHT!
(WEIGHT)
IViEIGHT)
(-EIGHT)
(weiGHT;
(hEIGHT)
(HEIGHT)
(HEIGHT)
(HEIGHT)
(l-EIGHT)
(V.EIGHT)
(V.EIGHT)
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7:15
8: 8
12: 8
14:32
7:15
3: 3
12: 8
14:32
8: E
12: c
14:32
HR.S
HRS
hRS
HRS
HRS
HRS
H^S
«?.s
hRS
H.RS
8: £ r"*S
-
-^
~
^
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si
=;
12: a
14:32
7:15
15:15
12:15
2C:15
hRS
H-;S
H.RS
HRS
HRS
HXS
143.00 HRS
A V E S A"
148.90 HRS
152.90 HRS
155.30 HRS
A V = R A
14S.CC i-P:S
A V E R A
148.90 HRS
152.90 HRS
155. 20 >-?s
A V E S i
I*.1:. SO *-^S
152.^0 rSS
155.30 HRS
A V E R A
152.50 'rSS
A '] = R A
i-'-3.CO HsS
156. CO HRS
A V ERA
153. CO HRS
iil.CO HRS
TOT
R A
K 2
tET)
G E :
SET)
(ET!
(ET!
G E :
(£T)
G £ :
«£T)
(2T)
C E :
; £- )
(ET)
(ET!
G E :
(£T)
?£T)
C, E :
C£T>
G E :
(ET)
iET)
A L :
T F. :
S GENERATOR /SUL
H2 CCNC- INLET GAS
\-Z CCNC INLET GAS
1-2 CCNC CUTLET EAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
F2 CCNC CUTLET GAS
N2 CCNC INLET GAS
N2 CCNC IKLET CAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
.":2 CCVC CL7LET GiS
.'<2 C~-v" CUTL-T GJS
H2S CCNC CL'TLST GAS
H2S CCKC CUTLET CAS
F2S CCKC CUTLET GAS
H2S CCNC CUTLET GAS
r20 CCNC CUTLET G.'-S
5-20 CCKC CUTLET GiS
H20 CC.'-C CUTLET GAS
H2Q CCKC CUTLET GAS
N2 IN:LET VCL FLCH RATE
"2 INLET VCL FLCr. P.ATE
N2 INLET VCL FLC'« RATE
WEIGHT CYCLCNE CLST
V.rlGHT CYCLCNE CL-ST
V.EI3HT CYCLCNH ELST
WEIGHT CYCLCNE DLST
FUR S
?GS-1CC! /
iGS-ICO! /
(GS-1C6) /
{GS-108! /
«GS-10S) /
(GS-1GS) /
(GS-iCO) /
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ON
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STATUS REPORT CF OPERATING CCNCITICNS FCR
r-: OPERATING PERIOD:
>: CATE: */2c/7A TlCt CF RECCRC: 7:1= H!
.1
- PRCCESS ELAPSEC TK'c CF PERIOD: START 14 =
r-.
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t 9. ACIO LCACIK-- INLET CARSCN 6" U.MT xsoic =
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I;
a 13. TOTAL AC'" CC\VFRTFD S» UMT PVC
jc; 1«. SULFUR CCNVcSSICN (TO H2S) PSCt-S =
C 15. SULfUR CCNCENSER EFFICIENCY £RV4CO«
n
; MATS FV=\TS CURING" CFERATING PERIOC:
Li "
CUT CN C02 TD 40 CFH IN 4" UMT AND
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U ATTEMPT TO TURN STEAM CN TO 4" UNI.I...AI ..
IXJ 150.3 !-*S. UNSUCCESSFUL DUb IU LKUlU.H^iO IN
\J STEAV LIME. ELEX SULFUR FRCV RfcCl^UULAI Ii-.^
4/26/7A PAG; 7
INTEGRATED OPERATION CF S02 RECCVERV PRCCESS ,
i
S TC 15:15 HRS
.r'-i VR<; / p\n i?&.co HRS LENGTH CF PERIOD: e.oo FRS .,
i
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56.03 ? (ACTUAL) 9C.O ? (GCAL) '>
57.80 Z (ACTUAL! "55. C 31 (GCAL)
il.99 % (ACTUAL) ??.C t (GCAL)
iC.90 ? (ACTUAL) 90.0 3 (GCAL)
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33.34 * (ACTUAL) 1CC.O S (GCAL) OF SCRBED S02
3C.75 3 {ACTUAL 3 25. C S (GCAL) CF STRIPPED SULFUR
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4/26/74
STATUS REPORT CF OPERATING CCNCIT1CNS FCP- INTEGRATED CPER4TICN CF S02 RECCVCRV PROCESS
PAGE S
r.
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OPERATING PERIOD:
CATE: 4/26/74 TIME OF RECCRC: 7:
PRCCESS ELAPSEC TIPc CF PERIOD: START
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HYCRCGEN MATERIAL BALANCE:
PACE 10
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".'LET _
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N.L.EJ
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£ R A T C
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HYCRCGEN/1-R
» ^
-------
APPENDIX A-12-11
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
RUN IR-2-8 (156 - 168 hours)
365
-------
PAGE
STATES REPCS.T CF OPERATING CCNCITIONS FC: INTEGRATED GPERATICN: CF SC2 RECCV'SY PROCESS
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OPERATING PERICC:
CITE: 4/26/74
CATS: <./ 27/74
PRCCESS ELAPSE: TIME
* .
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TIME OF RECCRC: 'C: 0 >-R3 TC 3'-15 HRS
*
CF PERIOC: START 15i.CC HRS / ENC 16S.CO HRS LENGTH CF PERICC: 12.00 HRS
i
PROCESS VARIABLES FCR CPERATING PERICD:
18:15 HSS
22:15 HRS
2:15 HRS
IS: 15 HRS
22:15 HRS
2: 15 HRS
15: 15 HRS
3: 15 HRS
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159. CO HRS (£T)
163. CO HRS !£T)
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AVERAGE:
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la 7. CO HRS
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161.00 HRS (ET)
164. CO HRS (ET)
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TOTAL :
RATE:
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163.00 HSS (5T>
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168. CO HRS !£T>
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RATE:
S C 2 SCR
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H20 CCNC INLET FLUE G SS
H20 CCNC INLET FLUE G =S
H20 CCNC INLET FLUE C SS
ORIFICE PRESSURE DRCF
CRIFICE PRESSURE DRC?
CRIFiCE PRESSURE CRCF
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
GRIP ICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
ViCIGKT CYCLCNf CUST
hrlGHT CYCLCNE CUST
WEIGHT CYCLCNE CLST
V.SIGHT CYCLC.\c DUST
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A/26/74
PAGE
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2:15 i-RS 167. CO US (ET! S TOT S CN IMLET CA?,!C\ (CS-3CU / Z30M1.T) =
AVERAGE: S TOT S CN INLET C1RICN (CS-3C1) / AZ3014 =
1<.:15 HRS 155. CO HRS (ET) ? H20 C.N INLET CARBC! (CS-3C1I / Z30H2.T) =
22:15 HR5 163.00 !-RS ( = T) % (-20 CN INLET CARECI. JCS-3C1) / Z3C1(2,T) =
2:15 HRS 167. CO HR5 (ET! % >-20 ON INLET CAREG!. ICS-3C1I / Z30K2.T) =
AVERAGE: t H20 CN INLET CASED! CCS-3C1) / AZ301E =
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3:15 HRS 168.00 HSS (ET) % TOT S CN CYCLCNE J.ST ( C-3C1) / C3CHI.T) »
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4/24/74
PAGE 4
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S02 CCNC CUTLET GAS
H2S CCNC INLET GAS
H2S CCNC INLET .G.' S
H2S CCNC. INLET GAS
H2S CCNC INLET GAS
H2S CCNC INLET GAS
H25 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H20 CCXC I^LET GAS
H20.CCNC INLET GAS
H20 CCNC INLET GAS
H2Q CCNC INLET GAS
H20 CCNC INLET GAS
H20 CCNC CUTLET GAS
H2C CCNC CUTLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
"J2 CONC INLET GAS
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24.100
23.400
23.300
23.300
49.600
49.600
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52.400
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53.2CO
53.950
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4/26/74
PAGE
H 2 S
GENERATOR/!. JLFUR
STRIPPER
17:15 HR
H2 CCNC INLET GAS
CO
16:20 H9S
19: 15 H1RS
20:24 HRS
21:38 HRS
17:15 HRS
16:20 r-?S
19:15 HkS
2C:2t HRS
£ !.- 2. >i r"^ S
0:15 HRS
1:15 rR S
3:15 HRS
16:20 HRS
19:15 HRS
20:2i HRS
3 i * "3 ;> ijO C
3: 15 HRS _
16:23 HRS
15:15 rRS
20:26 HIS
21:3= HRS
0:15 -RS
1:15 HRS
3:15 HRS
15:15 H.R3
3:15 HRS
20:15 hRS
3:15 HRS
20:15 HRS
3:15 HRS
14:15 HRS
15:15 HRS
22: 15 rRS
2:15 HRS
AVERAGE:'
157. 10 HRS (ET!
16C.CO H'RS !£T)
161. 2C HSS (ET!
162.40 HRS 1£T)
AVERAGE :
153.00 H"
TOTAL:
RATE:
161.00 HRS iET)
153. CO HRS (ET)
TOTAL:
RATE;
155.00 HRS (5T>
15S.CO H:'.S (ET)
16!. CO HRS !JT)
167. CO HSS tET)
!-2 CCNC INLET GAS
H2 CC\C CUTLST G4S
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
N2 CCNC I.NLET GAS
N2 CCNC INLET GAS
N2 CCNC CUTLET GAS
NZ CCNC CUTLET GAS
N2 CCNC CUTLET CAS
M2 CCK.C CUTLHT GAS
\!2 CCNC CUTLET GAS
N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET EAS
I-2S CCNC CUTLET GAS
t-?^ (" f* N: *~ f" ! ' T 1 P T f* fi %.
H2S CC.NC CUTLET CAS
H23 CCNC CUTLET GAS
H2S CCNC C'JTLET GAS
H2.S CCNC. CUTLET GAS _.
H2C CCNC CUTLET G&S
H2C CCNC CwTLET GAS
H2C CC.NC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CL'TLET GAS
N2 INLET VCL FLCX RAT£
;2 INILET VCL FLCV- RATE
iN2 INLST VCL FLCV. RATE
SvEIGHT CYCLCNE CLST
HEIGHT CYCI.CNE CLST
V.EIGHT CYCLCNE CLST
WEIGHT CYCLCNE CLST
WEIGHT FILTER CUST
WEIGHT FILTER CLST
WEIGHT FILTER CUST
HEIGHT FILTER CUST
3 TOT S CN CYCLCNc CLST
% TCT s CN CYCLCNS OLST
2 TC" S CN CYCLCNE CL£"
% TOT S CN CYCLCNE CLS'
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CGS-106! /
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C'C-S-IOS) /
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(GS-103! /
(GS-10S) /
(GS-10E) /
(GS-10E! /
rGS-lOE) /
iGs-ioai /
fi^C 1^31 /
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(GS-iO£! /
JGS-108! /
(GS-lCe! /
(GS-1021 /
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JGS-iCc! /
GS-ioa; /
(GS-10e) /
(GS-103) /
SGS-ioe: /
1SS-1C ! /
( G-1C ) /
! S-1C ) /
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< C-IC ) /
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! 2-10 ! /
t C-1G ! /
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{ 0-102) /
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Y1C3(5,T)
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C1C1U.T
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= 0.0 J ! VCL-JKE)
C.O ? (VCLUME)
C.050 ? (VCLUME)
51.500 S (VCLUME)
51.500 S (VCL'J."£)
56. COO ! (VCLC^E)
52.400 ? (VCLUX.E!
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53.2CO ? (VCLUMS1 .
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52.600 t (VCLUME)
53.571 ? (VCLU.Vc)
23.300 (VCLUME)
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22.400 (VCLUKEJ
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22.371 S (VCLUME)
127. OCO C?H (7C C=G F)
127.000 CFH (70 CEG F)
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0.0 12 CUST
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JLJCT_JS_?1_?1»J5
-------
4/26/7*.
PAGE
U>
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14-.ll
13:15
22:15
2:15
14:15
13:15
: 22:15
2:15
H.RS
HRS
HRS
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155. CO
159. CO
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157. CO
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163. CO
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CA^ECN RECYCLE RATE
CA33CN RECYCLE RATE
CiRSC\ RECYCLE RATE
( C- 90; /
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31.000
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-------
STATUS REPCRT OF OPERATING CONDITIONS FCR INTEGRATES OPERATION Cf SC2 RECOVERY PROCESS
CO
'
OPERATING PERIOD:
C6TE: 4/24/74 TIME CF RECCRC:
CATF: 4/27/74 TIX= 2F RFCCRC:
15:15 H
AS TC 24". 0 HRS
0: 0 h^S TO 3=15 HRS
.:
PROCESS ELAPSED TIKE CF PERIOD:
START 156
.CC hRS / END 166. CO rRS LENGTH CF PERICD: 12.00 hRS
SUHVARY CF INTEGRATED PROCESS PERFCRCANCE:
,
1. S02 RE.-CVAL
PRSC2 «
95.14 ? (ACTUAL) 90. C 31 (GCAL)
..
t
3
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r.
--
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3. AC 10 CCNVERSICN I TO SULFUR)
4. (-2 LTILIZATICN ( TC H2S)
5. SULFUR RECOVERY
6. (-2 UTILIZATION V U'HT
PU!-2S *
PVCS =
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PRS
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ICC. CO S (ACTUAL! 95. C ? (GOAL)
63.69 % ? ACTUAL! 99. C 5 (GCAL)
62.46 * (ACTUAL) SC.C S (GCAL)
88.08 % (ACTUAL) 1CC.C S (GOAL) CF SCR3EC SC2
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3. CAR5CN RECYCLE RATE (DB)
?. ACID LCACING I\L=T CARECN 6" UNIT
1C. XCMSTURE CONTENT INLET CAR3CN 6" UNIT
11. ACID LCACUiC- INLET C«ECN 81: Ur: I T
b2. ."Q! STL-RE CONTENT T.NLET CARBON 8" UNIT
13. TOTAL JCIC CONVERTED 8" UNIT
1*. SULFLR CC^VE?3iC^f 1 "C- *2S S
i?. iLiFLS CCN--ENSER EFFICIENCY
X9CA =
RC90 *>
X3C1C =
X301S =
X3C2C =
X3023 =
PVC =
PSCi-S =
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C.C431 LS S/LE C
Zfi.917 LB C«DE5/HS
C.2159 LB ACIC/L3 C
C.C932 L3 P2C/LE C
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f'j- c"? cc2 TC »' u>;r~ :
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STATUS SzPCRT CF OPERATING CCNCITKNS PCS INTEGRATED GPER2TIC.X C? SC2 RECCVERY PROCESS
CO
OPERATING PERIOD:
futfi 4/2t/?4 TIVE QF RECCRC: 15:
CATE: 4/27/74 T;*E Of RECCRC: o-.
PRCteSS SLAPSEC TlYE CF PERICD: START
SULFUR MATERIAL BALANCE (USING PROCESS h2S):
S 0 2
I N
INLET GAS AS S32
INLET C AS PESIDUAL S
T C T A L IN:
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CUTLET GAS AS SC2
CUTLET CiRSOi
CYCLCKE CUST
CCLLECTCR OUST
CtReCfv V,EE?AG£
TCTAL CUT:
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!.\LET GAS AS r2S (PftCC)
INLET CiR3CfJ
T C T A I IN:
CUT
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CUTL3T US ii SC2
CUTLET C-3.-,CN
T C T i L OUT:
15 HRS
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156. CC
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TOTAL OUT:
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INLET GAS 8" UNIT AS CVL H2S
TOTAL
CUT,
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<./26/74
PAGE 12
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APPENDIX A-13
DATA FROM SOLVENT EXTRACTION EXPERIMENTS
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-------
APPENDIX A-14
LITERATURE SURVEY FOR RECOVERY OF SULFUR
BY SOLVENT EXTRACTION
I. SULFUR RECOVERY - REVIEW ITEMS
1. Berthelot, Ch. Recovery of sulfur in the coke plants in Germany.
Genie Civil 113, pp. ^01-6 (1938).
2. Berthelot, Ch. Recovery of sulfur in coal-carbonization plants
and petroleum refineries. Genie Civil 116, pp. 6-7 (19^0).
3. Brabant, M. Desulfurization of (town) gas and sulfur recovery
processes. J. usines Gaz 6k, pp. 33-^3, ^9-56, 69-75 (19*4-0).
k. Brabant, M. Desulfurization of gas and processes for recovery of
sulfur. Schweiz. Ver. Gas-u. Wasserfach. Monats-Bull. 21, pp
26-30, Ul-2, 96-100,
5- Bulian, W.; Dittmar, A., and Feher, F. Removing elementary sulfur
from natural gas. Erdoel Kohle, Erdgas, Petrochem. 20 (12),
pp. 849-52 (1967).
6. Evans, E. C. et al-Special study of sulfur removal and recovery
from fuels. J. Inst. Fuel 29, pp. 138-9 (1956) .
*7« Goar, B. G. Today s sulfur recovery processes. Hydrocarbon Process.
1968, U7(9), PP. 2^8-52.
8. Grosskinsky, 0. Recovery and utilization of nitrogen and sulfur pro-
duced in coal carbonization. Bergbau - Arch. 5/6, pp. 1^6-52
(19^7) .
*9. Kronacher, H. K. Modern Desulfurization Processes in Germany.
Gas-Age Record 68, (2), pp. 37-56 (1931)-
* Filed in Charleston Research Center
Translated into English
388
-------
10. Lissner, A. The importance of the sulfur of coal in the German
raw-material economy. Tech. Niederdonau 1, 197-9, 218-21
*11. Lorenzen, G. Purification of Gases with Special Attention to
Desulfurization and the Recovery of Sulfur. Chem. Fabrik
12(1,2) :6-23 (1939).
12. Muhlert, F. Recovery of by-product nitrogen and sulfur in the
coke-oven and gas industries. Brennstoff-Chem., 10, pp. 1*87-
90 (1929).
*13. Powell, Alfred R. Recovery of sulfur from fuel gases. Ind. Eng.
Chem. 31, PP- 789-96 (1939)-
14. Rosendahl, F. Recovery of coke-oven gas products. Oel u. Kohle
ver. Petroleum, 36, pp. 229-^3 (19^0).
15. Secchi, I. M. Recovery of sulfur from coke-oven gases. Chim.
e industria (Italy) 19, 187-91 (1937).
*l6. Sweeney, E. L. and Sands, A. E. The removal of free sulfur
from spent oxide. Gas Age - Record 779 pp. 657-62 (1936).
17. Thau A. Extraction and utilization of fuel-gas sulfur. Z. Ver.
deut. Ing., Beiheft Folge 1938, no. 3, pp. 8l-6.
18. Wagner, P. Utilization of spent oxide from gas works. Rev.
Prod. Ghim.,.2U, pp. 397-^ (1921).
389
-------
II. SOLVENTS FOR SULFUR EXTRACTION
A. Ammonium Compounds
1. Aoki, T.; Morikawa, M. and Akiyama, Y. to Sumitomo Chem.
Co. Recovery of sulfur from hydrogen sulfide. Japan
patent 582,626. April 12, 1958.
2. Collin, F. J. A-G. Extraction of sulfur from fumes con-
taining hydrogen sulfide. British patent 7^8,037-
April 18, 1956.
3. Gluud, W., Schonfelder, R. and Riese, ₯. Purification of
sulfur from gas plants. Brennstoff-Chem. 8, pp. 168-9
(1927).
^- I. G- Farbenind. A-G. Gas purification. British patent
320,190. Aug. 25, 1928.
5. Pieters, H. A. J. Removal of hydrogen sulfide from gases.
Brennstoff-Chem. 18, 373-6 (1937).
6. Wallis, E. Recovery of sulfur in a marketable form from
flue gases. Brit. Chem. Eng. 7, pp. 833-6 (1962).
7. Williams, P. E. Treatment of spent oxide. British patent
596. Jan. 9, 1909.
B. Aliphatic Hydrocarbons and Derivatives
1. Alexander Wacker Gesellschaft fur electrochemische Industrie
G.m.b.H. Recovering sulfur from used gas-purifying
masses. Brit, patent 508,966. July 7, 1939.
2. Bonner, L. C. Treating gas purifier. British patent 10,780.
May 1,
3. Every, R. L. and Grimsley, R. L. to Continental Oil Co. Pre
paring dispersable sulfur. U. S. patent 3,318,666.-
k. Genther et Franke. Extraction of sulfur. French patent
377,82*1. May 15, 1907-
390
-------
5. Muszkat, K. Production of free sulfur from hydrogen sul-
fide-absorbing materials in the Warsaw Gas Works. Gas i
Woda 17, pp. 235-8 (1937).
6. Roga, B. Gas purification masses as a source for the re-
covery of sulfur. Przeglad Gorniczo-Hutniczy 30, pp.
i+32-6 (1938).
7. Simpson, C. H. Extraction of sulfur from material contain-
ing elemental sulfur. U. S. patent 3,063,817. Nov. 13,
1962.
8. Stobe, R. Reclaiming sulfur from the mass used for gas
purification. German patent 708,031. June 5,
C. Aromatic Solvents
1. Anon. Recovery of the sulfur from spent oxide. Gas World
57, 197 (1912).
2. Becigneul, J. Obtaining sulfur from gas-purifying materials,
U. S. patent 833,573. (1907).
*3. Bradley, G. W. and Barritt, D. T. Sulfur. British patent
72^,119. Feb. 16, 1955.
k. Germogenova, E. V. Utilization of mixed solvents for the
extraction of sulfur from sulfur ores. Mineral. Syr'e
1937, no. 5, pp. 28-35.
5. Herold, P. to I. G. Farbenind. A.-G. Purifying coke-oven
gases, etc. German patent 570, M*8. Sept. 26, 1928,
6. Hunt, E. J. and Glidden, W. T. Recovering sulfur from
tarry spent oxide. U. S. patent 105,996- April 29,
1913.
7. Jaeger, A. Sulfur extraction from spent gas-purification
using tetralin (and low temp, tar oils). Brennstoff
Chem. 3, p. 356 (1922).
391
-------
8. Katewinkle, R. Recovery of sulfur from spent oxide by
means of tetralin. Brennstoff Chem. 3, PP« 310-1
(1922).
9. Kuster, 0. R. to Lummus Co. Continuous counter current
crystallization. U. S. patent 3,337,30?. Aug. 22,
1967.
*10. Prchlik, J. ; Hlinak, L. and Kartakova, C. D. Recovery of
sulfur from spent gas works purification mass. Paliva
3U, PP. 298-305 (195*0.
11. Rosen, R. to Standard Oil Dev. Co. Removal and recovery of
free sulfur from gas -purification materials, etc. U.
S. patent 2,195,870.
12. Soc. d Eclairage, Chauffage et Force Matrice. Removing
sulfur and nitrogen from exhausted gas-purifying mass-
es. French patent
13. Suru, J. The desulfurization of gases. Technikai Kurir 8,
pp. 31-2 (1937).
1^. Weil, J. A. to Imperial Industries Ltd. Sulfur. British
patent 561,370. May 17, 19^.
15. Wohlwill, M. to Metallgesellschaft Akt.-Ges. Reclaiming
sulfur from gases. German patent 707,132. May 15,
D. Organic Sulfur Compounds
1. Anderson, W. Cyanogen compounds; sulfur. British patent
127,128. June 15, 1918.
2. Capell, R. G.; Wright, J. H. and Cruse, Wm. A. to Gulf Re-
search and Dev. Co. Recovery of elemental sulfur from
sulfur-bearing solid mineral matter, u. S. patent
2,897,065. July 28, 1959-
392
-------
3. Chemische Fabrik Phonix, Rohleder and Co. Recovery of
sulfur from extracts of gas-purifying masses. German
patent 182,820. Nov. 16, 1905.
k. Deal, Carl H. and Papadopoulos, M. N. to Shell Oil Co. Re-
moval of sulfur-containing gases from gaseous mixtures.
U. S. patent 3,363,989. Jan. 16, 1968.
*5. Potsdamer, L. S. Notes on sodium prussiate. J. Ind. Eng.
Chem., 11, pp. 769-70 (1919).
6. Strauss, F. to Gottfried Bischoff K.-G. Extraction of
sulfur-containing materials. German patent 1,1^7,566.
Apr. 25, 1963.
7. Strauss, F. to Gottfried Bischoff K.-G. Recovery of sulfur
from gas purification masses. German patent 1,131,192.
June lU, 1962.
E. Other Organic Solvents
1. Johnson, E. J. A theory of fluidization and its applica-
tion to sulfur recovery by solvent extraction. Inst.
Gas Engrs. Publication no. 378 (a), 39 pp. (1950).
2. Murphy, E. J. Removal of sulfur from spent oxide. J. Gas Lighting
136, pp. 396, pp. 396-7 (1916).
3. Sawa, M.. to Nittetsu Mining Co., Ltd. Crystallization of sulfur in
solvent refining. Japan patent 6318,207. Sept. lk, 1963.
393
-------
III. USE OF ACTIVE CARBON IN SULFUR RECOVERY FROM GASES
1. Bakes, W. E.; King, J. G. and Sinnat, F. S. Sulfur compounds in
water gas and their removal. Dept. Sci. Ind. Research, Fuel Re-
search, Tech. Paper 31, 35 pp. (1931).
2. Braeuer, H. ₯.; Rogge, K. Natural gas refining by desulfurization
with active charcoal. Erdoel, Erdgas Z. 1967, 83(5), PP- 170-8.
3. Brychta, M. Separation of sulfur from Lurgi generator gas. Paliva
36, pp. 391-9 (1956).
k. Carbonisation et charbons actifs. Desulfurizing gases. British
patent k79,klO. Feb. k, 1938.
5. Englehardt, A. Use of active materials at coke ovens and gasworks.
Glukauf 73, pp. 925-33 (1937).
* 6. Fischer, F. and Kloeckner, L. New method for the purification of
viscose exhaust air. Wasser, Luft Betr. 10(12), pp. 833-5 (1966).
* 7. Grantham, L. F.; Larsen, C. M. to N. American Rockwell Corp. Sulfur
production from flue gases. U. S. patent 3,^38,733.
8. Griffiths, H. Activated carbons-modern applications for adsorptive
processes. Chem. Trade J. 96, pp. 235-6 (1935).
9- Hoffman, Th. New methods and goals in desulfurizing illuminating gas.
Chem. App. l6, 6l-63, 120-1 (1929).
10. Rollings, H. and Evans, E. V. Report on removal of sulfur compounds
from town gas down to 10 grains per 100 cubic feet. Institute of
Gas Engrs. Pub. no. 1^6/^3, 21 pp. (1936).
11. Knauf, G. Application of activated carbon for sulfur removal in gas
purification. Energietechnik 1968, 17 (ll), pp. 14-85-8.
394
-------
*(T)12. Koenigstuhl, M. D. Extraction of sulfur from the hydrogen sulfide
of coke-oven and other gases by means of activated charcoal.
Coke and Chem. (U.S.S.R.) 1932, no. 7, pp. 32-7.
13- Kostrikov, V. I.; Keltsey, N. V., and Nivin, P. I, Use of one
sorbent to remove both hydrogen sulfide and carbon disulfide
from rayon-industry waste gases. Khim. Volokna 1968(2).
l4. Krczil, F. Catalytic oxidation of hydrogen sulfide in presence of
active carbon. Chem.-Ztg. 6l, pp. 2*4-7-8, 2^9, 267-8, 269-70
(1937).
15. Metallgesellschaft A-G. Removal of hydrogen sulfide from gas mix-
tures. French patent 1,388,^53. Feb. 5, 1965.
16. Weuwirth, F. Desulfurization of gas with Koflach lignite charcoal.
Berg-u. Huttenmann. Jahrb., 76, pp. 1-13(1928).
17. Stanisz, Z. Regeneration of sulfur from gases by means of activated
charcoal. Przeglad Chem. 2, pp. 530-1 (1938).
18. Thoma, M. Fine purification of gas. Schweiz, Ver. Gas-u. Wasserfach.,
Monats-Bull. 16, pp. 257-68(1936).
19. Todd, E. W. Removal of sulfur from illuminating gas by activated
carbon. Nova Scotian Inst. Sci., 17, Pt. 2, pp. 12-3 (1928).
20. Visconti, Y. S. Obtaining elementary sulfur. Rev. brasil. guim.
(Sao Paulo) 22, pp. ^15-18(19^6).
*(T)21. Waeser, B. Desulfurizing gases. Chem.-Ztg. 52, pp.. 617-8, 638-Uo,
658-9 (1928).
395
-------
IV. SOLVENT EXTRACTION OF SULFUR FROM CARBON
A. Ammonium Sulfide
*1. Comm. on Gas Mfg. of the Assoc. Technique. Gas purification
by activated carbon and recovery of sulfur in the solid
form. Gas Journal, 184, pp. 526-7 (1928).
*(T)2. Egorov, N. N., et al. Purification of gases with activated
carbon. Chapter IV, pp. 37-47 of "Removal of Sulfur
from Coke-Oven and Other Fuel Gases," Moscow, 1950.
*(T)3. Engelhardt, A. The use of active charcoal in the gas in-
dustry. Gas-u. Wasserfach 71, pp. 290-7 (1928).
4. Evans, K.; Pearson, H. P., and Reisemann, E. Industrial
Applications of Active Carbon. Trans. Inst. Chem. Eng.,
Dec. 6, 1929, pp. 62-83.
5. Gouthiere and Co., and Ducanel, P. Recovery of sulfur from
used gas-purifying masses. Ger. Patent 245,570. July 14,
1910.
6. Kazarnovskii, S. and Pisarev, K. The purification of gases
from hydrogen sulfide by oxidation on activated charcoal.
J. Chem. Ind. (Moscow) 12, pp. 913-21 (1931).
7. Prchlik, J. Removal of active carbon of sulfur from waste
gases obtained during production of town gas in the Lurgi
generator. Prace Ustavu Vyzkum Paliv 1963(6), pp. 138-50.
8. Reichert, 0. and Stemmler, H. to Spinnfaser Akt.-Ges. Recovery
of sulfur from activated filter charcoal. Ger. patent
1,054,655. April 9, 1959-
*(T)9. Spechal, W. Sulfur removal from synthesis blue gas by active
charcoal. Gas-u-Wasserfach 94, pp. 679-8U (1953).
10. Szilagyi, I. Method to purify and to remove sulfur from the
raw gases produced.from lignite. Magyar Kern. Lapja 4,
pp. 24-5 (19^9)-
396
-------
11. Tyulyukov, A. and Khronova, M. The purification ol' gasen con-
taining hydrogen sulfide by active charcoal. J. Chem.
Ind. (u.S.S.R.) 12, pp. 2^7-5^ (1935).
12. Zel'venskii, Ya. D. and Volkov, A. E. Gas purification from
hydrogen sulfide by oxidation on active carbon. Trudy
Gosudarst. Nauch.-Issledovatel. i Proekt. Inst. Azot.
Prom. 1952, no. 1, pp. 131-8 (1953).
B. Organic Solvents
1. Becigneul, J. J. M. Extracting sulfur from spent gas-
purifying materials. Brit, patent 9»800.
*2. Braeuer, H. W. and Fischer, F. Recovery of carbon disulfide
with simultaneous removal of hydrogen sulfide. DECHEMA
monograph 1968, 59(10^5-1069), 173-89.
3. Brychta, M. Desulfurizing coke-oven gas by activated carbon.
Prace Ustavu Vyzkum Palio 1962(U), pp. 169-232.
U. Cornillaux. Extracting and purifying sulfur. French patent
353,932, March 25, 1905.
*5. Fischer, F. and Kloecker, L. to Pintsch Bamag A.-G. Process
of regenerating activated carbon saturated with hydrogen
sulfide and an organic solvent present in exhaust air or
oxygen-containing gases. German patent 1,259»8U5,
Feb. 1, 1968.
*6. Riedl, R.; Brychta, M., and Praskova, D. Regeneration of spent
activated charcoal used for the adsorption of hydrogen
sulfide from pressure gas by toluene and xylene. Sv.
Vyspke Skoly Chem.-Technol. Praze, Oddil Fak. Technol.
Paliv Vody 3, no. 1, 5-3^ (1959).
*7. Schreiber, F. Use of tetralin in sulfur recovery from active
charcoal used for gas purification. Brennstoff-Ohem., 3,
PP. 355-6 (1922).
397
-------
APPENDIX A-15
S02 ACTIVITY AND PORE VOLUME DETERMINATION
OF SOLVENT EXTRACTED CARBON
Page
1. S02 Activity of Solvent Extracted Carbon 399
2. Surface Area and Pore Volume Distribution of 420
Solvent Extracted Carbon
398
-------
APPENDIX A-15-1
S02 ACTIVITY OF SOLVENT EXTRACTED CARBON
399
-------
GRAVIMETRIC PLOW EXPERIMENTS
RUJI:
Dry Weight:
Dol'lnction:
Carbon :
3 2' Mi
<>'j. 'i2 me.
2t
> ' "',: -
2000 ppm
EXV-1
NO:
02:
H20:
t:
0 pt>m
6p
200° F
FL:
3500 c-c/min.
76.66
Correction: 0.5007
Date: March 23, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
32
A
:tf
!H
40
42
44
46
liff
r>0
52
54
56
58
(,0
>'<'>
70
Load
nig. HaSOl|/g. C
6.57
8.86
10.63
11-99
13-34
14.80
16.26
17.83
19 . 50
21.37
23.04
24.92
26.64
28.67
30.65
32.74
34.82
36.80
38.99
41.18
43.27
45.45
47.96
50.25
52.65
54.94
57.44
60.05
f.2.55
65.05
f.9.85
75.06
79.86
Ml). 97
»')-VV
<)4.'*7
]00.t>8
10'l.lM
110.51
115.1-2
120 . 52
125. 7 S
JSO.M4
lv'..05
l4l.2»
15^.2'-
]..',. 24
Mean Load
tng. HgSOii/g. C
if
6
8
10
12
lit
16
18
20
25
30
35
4o
45
50
55
60
65
70
75
80
85
90
95
100
110
120.
130
i4o
150
160
170
180
190
200
220
21+0
260
280
300
320
3!tO
360
380
Rate
mg. %30^/g. C/min.
4.3520
3-5446
2.4395
1.6681
1.3553
1.4283
1.5325
1.6264
1.7098
1.8766
1.9912 '
2.0955
2.1789
2.2623
2.3249
2.387^
2.4291
2.4708
2.5021
2.5334
2.5542
2.5751
2.5959 '
2.6063
2.6063
2.6063
2.6063
2.5959
2.5646
2 . 5229
2.4917
2.4500
2,'WK
2.335-1
2.2621
2.1268
1.9808
1.8140
1.6785
1.5221
1.3866
1.2198
1.0530
0.8862
400
-------
GRAVIMETRIC FLOW EXPERIMENTS
(CONTINUED FROM PREVIOUS PAGE)
Run:
Dry Weight:
Deflection:
S02:
Carbon:
129- G
95-92 nig.
-2.53 rag.
2000 ppni
EXV-1
NO:
02:
H20:
t:
0 ppm
3-5$
ft
200° F
Ft: 1500 cc/min.
$ HgSO^: 76.66
Correction: 0.5007
Date: March 23, 1971
Time
minutes
75
80
85
90
95
100
io(;
110
115
120
125
130
135
ikO
11*5
150
155
160
165
170
175
180
185
190
195
200
205
2.10
215
220
Load
nig. HgSOij/g. C
177.33
188.70
200.17
211.53
222 . 58
21'«.11
2k 1 . 12
252.92
26.1.78
270.5l|
278.77
286.80
291*. in
301.1*0
308.38
315.16
321.52
327.88
33^.2U
3'*0.60
3't6.61t
352.90
35«.53
361). 16
369.58
37^.90
VfH.W
.VM.W
Wf.'jl
391-37
401
-------
GRAVIMETRIC FLOW EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
130-0
101.7U mg.
-2.55 mg.
2000 ppm
EXB-1
HO: 0 ppm
02: 3-5*
HgO: 6%
t: 200°F
1500 cc/min.
76.66
Correction: 0.5019
Date: March 2k, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
30
12
ll)
16
18
20
22
2U
26
28
30
35
l»o
1*5
50
55
60
65
70
75
80
85
90
9';
300
110
120
330
3 >(0
350
160
170
180
390
KOO
. 210
220
2'jO
«l|0
,"'.>0
i'M
."70
280
'f III
iuo
110
:«o
H'J
Ixsad
m«. H2SOl,/g. C
5.11
5.90
6.39
6.88
7-37
7.76
8.16
8.li5
8.85
9.2't
9-93
10.52
11.21
11.89
32.68
13.37
llt.3.5
Il4.8lt
15-73
16.51
18.58
20.71*
22.90
25.3.6
27.1*2
29-98
32. Ok
35-29
37.81*
110.59
1*3. Mt
'16.29
1*9.31*
52.29
58.1*8
6k. yr
71-95
79-12
86.30
93-28
100.65
108.12
115.1*9
122.76
129. 61|
136.52
I'l.-i.llO
]50.(M
.156.67
11,2.77
I6((.'i,,
17li.5t,
lllu. ',i,
J»5.77
J'M .17
Tlh.2!)
20.1 . 30
Mean Load
mg. H2SOl4/g. C
1|
6
8
10
32
3.1*
3.6
18
20
25
30
35
1*0
'5
50
55
60
65
70 ,
75
80
85
90
9'J
100
110
120
130
l'*0
150
3.60
170
180
190
200
Rate
rag. HgSOlj/fi. C/min.
. 3.M'><>3
0.5» 17
0.31(1)0
0.32!i'i
0.33'(2
O.Vi'tO
0.3M7
0.38.-M
o. 1*128
o. n5.2i
O.liyl'*
0.5 '308
0.5701
0.5<>9n
0.6291.
0.6'ib7
0.66?U
0.6t3o
O.i>,'7>)
0.7077
0.7175
0.7175
0.7273
0.7273
0.7273
0.7175
0.7077
0.^979
0. 66S.lt
0.6W?
0.6291
o.wv;
0.5/01
O.^liO'i
0.5011
402
-------
GRAVIMETRIC
Run:
Dry Weight :
Deflection :
S02:
Carton :
131- G
102.52 mg.
-2.1*5 rag.
2000 ppm
EXV-2B
NO:
02:
t:
0 ppm
3.5*
200* F
FLOW EXPERIMENTS
*v
1500 oc/min.
Correction: 0.1*851
Date: March 25, 1971
Time
minutes
1
2
3
1*
5
6
7
8
9
10
12
ll*
16
18
20
22
21*
26
28
30
35
1*0
1*5
50
55
60
65
70
75
80
85
90
95
100
110
120
330
Jl|0
150
.160
370
180
1^0
2
l.Y'l.70
183.38
.191.. 57
l<)<>.',7
207.76
;M',.57
2J2.98
230.10
2.16.H3
21*3.27
2l(9.)(l
255-56
261.1*1
266.68
Mean Load
mg. HgSOl^/i;. C
1*
6
8
10
12
ll*
16
18
20
25
30
35
1*0
1)5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
ll*0
150
160
170
180
190
200
220
21*0
260
Rate
mi-. H2SOl|/r- C/rain.
7.5595
U.8771
1.7070
0.5365
0.5365
0.51162
0.5560
0.5657
0.5755
0.61U5
0,61*38
0.6730
0.7121
0.71*13
0.7603
0.8096
0.8369
0.;V,6l
p. «97l*
O.yi69
0.9H61*
0.9559
0.9-'5'7
0.9852
0.991*9
l.OlWt
1.02l(2
1.021*2
1.021(2
1.001*7
0.9751*
0.91*62
0.9071
0.668:
0.81911
0.7316
0.61(38
0.5'»62
'
403
-------
Run:
Dr.y W.'ir.ht.
C-it-l on:
101 .'/O mi1;.
-3.74 u\i'..
li'KX) ppm
KXB-2
NO:
II20:
0 ppm
V//,
r/
200°F
1500 cc/niln.
72,06
Corroi-tlon: 0.4706
Date: March 30, 1971
Time
minutes
]
2
3
4
5
6
7
8
9
10
12
14
16
18
20
22
24
26
28
30
35
40
45
50
55
60
65
70
75
80
85
90
9'J
100
110
J20
no
I'lO
.1^0
JnO
.170
1 :'.<>
I'KI
2OO
21'.)
220
230
240
2'jU
2'.0
2/0
i'.".0
Lofid
mg. IlgSO^A;. C
8.44
9-13
9.r>2
9.81
10.40
10.79
11.09
11.38
11.68
11-97
12.56
13-25
13.94
14.62
15.21
15.90
If.. 68
17-27
18.06
18.84
20.71
22.67
24.63
26.59
28.56
30.52
32.58
34.74
36.80
38.96
41.22
43-57
45.83
4;-i.i8
'-!.. I')
',.'..-<>)
M.Y',1
f.('.2B
74 .'iM
:;().:/,
'-<..'!'>
".;.i.'i
'i.'.'M
j ( <* . >;>
IC". "1
31',.U
IL'O.'K'
12... SO
i-'.j. ;-
ny.'>°.
J.4 -i . .J,^
r4.(.;'7
Mean Load
mg. H2SOj+/g. C
It
6
8
10
12
Ik
16
18
20
25
30
35
4o
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
lltO
Rate
mg. HgSO^/g. C/isin.
8.6850
5-6919
2.3553
0.3925
0.3435
0.3435
0.3435
0.3533
0.3631
0.3925
0.4220
o.44i6
0.1*612
0.4809
0.5005
0.5201
0.5299
0.5397
0.5^96
0.5594
0.5692
0.5790
0.5888
0.5888
0.5888
0.5888
0.5888
0.5790
0.5692
404
-------
Run:
Dry Weight:
Deflection:
S02:
Carbon:
GRAVIMETRIC FLOW EXPERIMENTS
NO:
33't-G
99.98 mt;.
-2.83 my.
2000 ppm
EXV-2C
0 ppm
3.5?,
200° F
Ft:
1500 cc/min.
7!*.77
Correction: 0.1*883
Date: April 12, 1971
Time
minutes
1
2
3
l*
5
6
7
8
9
10
12
lit
16
18
20
25
30
35
1*0
U5 l
50
55
60
65
70
75
80
85
90
95
100
110
120
130
lUO
150
.160
170
JBO
190
200
2K)
2HO
230
2'tO
250
?/<0
270
280
200
300
Load
mr,. HgSO^/g. C
32.I|0
13. yo
l't.90
15.90
16.90
17.90
18.80
19.80
20.80
21.90
23.90
25.91
27-91
29.91
31-91
37.11
te.31
^7.71
53.01
58.61
61*. 31
70.11
76.02
81.92
88.02
93-92
99.82
105.92
111.92.
118.12
12l*.12
135-93
I't7.53
158.83
169.93
iHo.yi*
i<):i..6i*
20.1. 9'*
,2.11.9'*
221.5')
2 -|i ).8';,
2-tO.tf';
2'iM.lO
2'..(..'i')
Ht'Ji.lfi
272.05
27').jr,
2H5.06
2',«.66
209. l/,
30'). 26
405
Mean Load
mg. HgSOtj/g. C
6
8
10
12
11*
16
18
20
25
30
35
1*0
i*5
50
55
60
65
70
75
80 '
85
90
95
100
. 110
120
130
ll*0
150
160
170
180
190
200
220
2l*0
260
280
300
'
Rate
mg. HgSO^/g. C/min.
12.2525
9.5019
6.7511)
3-1*507
1.1002
1.0002
0.9902
0.9902
1.0102
1.01*02
1.0602
1.0802
1.1002
1.3202
1.1302
1.1502
1.1602
1.1802
1.1902
1.2002
1.2002
1.2102
1.2102
1.2102
1.2102
1.2102
1.2002
1.1902
1.1602
1.11*02
1.1102
1.0902
1.0502
1.0202
0-9502
0.8702
0.8002
0.7101
0.6201
-------
i; li A V I M K T li I C !' 1 0 W K X I' M R J M K N T !5
Hun:
Dry Weight:
Deflection:
S02:
Carbon:
lOO.H* mg.
-5-53 mg.
2000 ppm
EXV-3B
NO: 0 ppm
HgO: 6%
t: 200°F
Ft:
Correction:
Date:
1500 cc/min.
77. OU
0.5031
May 1*, 1971
Time
minutes
1
2
3
li
5
C
7
H
9
.10
\?
Ill
16
18
20
25
30
35
140
U5
50
55
60
65
70
75
80
B5
no
."10
;>?o
: -;o
;-'iO
Load
:r:G. llgSO^/g. C
6.09
7-39
8.29
9.. 19
10.19
:n .08
K',08
.13.08
Hi. OH
J5.08
17. ?8
19. W
. 21.77
2^.07
26Ji6
32.75
39. 7U
^7-23
55-12
63-i+l
71.50
79.79
88.18
96.56
105.25
313.7li
122.1.3
.130. IIP
.138.51
.1)16.60
15)1.38
169.66.
lH)i . Di
.197.82
2.10.80
223.19
235.17
2)16.^5
257. OH
^if.7.0?,
27''». 21
?;>i.yo
292 . w
>3VY
.1 . (",038
1 . 55?8
1 . 5029
l.kk&O
1.3980
1.31 (31
1.2283
l.l]8)i.
1.0036
0.8838
0.7639
406
-------
C, K A V I M K T R I C FLOW EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
H47-G
103.3 nig.
-5.26 mg.
2000 ppm
EXB-2
NO:
02:
HgO:
t:
0 ppm
200°
Correction:
Date:
1500 cc/min.
76.11
0.14970
May 6, 1970
Time
minutes
1
2
3
It
5
6
7
8
9
10
12
l!|
16
18
20
25
30
35
40
't5
50
55
60
65
70
75
80
85
90
95
100
3 10
320
.130
:iiio
150
.160
170
J8o
i_yo.
poo
210
?20
230
PUO
Load
ing. H2S01|/g. C
li.26
5.52
6.29
6.97
7-65
8.23
8.81
9.ii9
10.07
10.711
.12.00
13.36
l)i. 81
16.16
17 -.62
.21.20
2)4.97
28.9't
32.81
37.07
l»l.62
k6.U6
51.78
57-10
62.62
68.23
7h. ll)
.80.33
86.53
9?. 82
99.?1
:n?.?7
:ip:..f«:
!;!«. 99
35J -86
l6li.)|)i
r/A.)|)i
i ' ' '. ) -pi
!<:>, ) )
1 ' )<).>'/>
PI 1.1 9
;>:;'. 13
>",:?. 68
^ij.ox
253.. 19
r6P.it 9
Mean Load
mg. HgSOj^/g. C
2 n
k
6
8
10
... 12
Ik
16
18
20
25
30
35
1)0
)i5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
l!|0
.150
160
.170
180
190
P.OO
??Q
P)|0
:-'6o
Rate
mg. li^SO^/s. C/:ain.
k. 355^
2.14.003
0.77^3
0.6775
0.6581
0.658.1
0.6630
0.6727
0.6872
0.7065
0.7598
0.8227
0.8808
0.9388
0.9872
i.0308
1.07^3
1.1130
1.1518.
1.1905
1.2292
1. 2W5
1.2679
1.2873
1.2969
1 . 3066
1.3163
1.3163
l . 3066
1.2969
1.2776
1.2582
1.2389
1.2098
1.1808
.1 .1518
.1.0889
] .()!(>{
Q.<)WV,
407
-------
GRAVIMETRIC FLOW EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon :
154-G
117.04 mg.
-5-53 mg.
2000 ppm
EXA-1
NO:
02:
HjO:
t:
0 ppm
200 °F
!t!
Correction:
Date:
1500 cc/min.
71.24
0.4652
May 26, 1971
Time
minutes
1
2
3
)|
5
6
(
0
9
JO
.1?
14
16
18
20
25
30
35
40
45
50
60
70
80
90
:ioo
.110
.IPO
J'J,0
I'lO
11)0
160
.170
180
190
?00
?10
220
?30
?l|0
250
tf>0
270
r.".o
?' )0
"<00 j
Load
r,ie. H2S01(/g. C
0..17
0.34
0.60
0.77
0.94
.1 . .1 1
1.37
.1 . 5'i
1.79
1.97
2.31
2.73
3-08
3.42
3-67
4.53
5-30
6.07
6.75
7-43
8.03
9.31
10.li2
11.53
12.65
13.67
.Hi. 70
_Lk- 5>
1 6 . V
l/.oy
jy.f")
18.37
39.22
20. ?'j
21 . 36
22.73
2)|..l8
25-72
27-17
28.96
30. y>
3?.3U'
3'i.l»
3«i. 'V.
:;7.M.'i
;'».fl,"
Mean Load
mg. H^SOj/g. C
2
It
6
8
10
-, 12
:4
16
18
20
22
24
26
28
30
3?
34
36
38
40
Rate
mg. HgSOjj/g. C/min.
0.2153
0.1692
0.1393
0.1?56
0.1128
0..1008
0.0897
0.0705
0.0880
0.109)1
0.1282
0.1427
0.1521
0.1623
0.1692
0.1777
. .0.1837
0.1897
0.1931
0.1965
^
408
-------
0 R A V 1 M !; T K I C F 1, 0 W EXPERIMENTS
Run: J5'j-G
Dry Weight: 108.52 mg.
Dofleetlon: -5-85 mg-
2000 ppm
D02:
Carbon:
NO: 0 pprj
02= 3-5V
200°?
Ft:
Correction:
Date:
1500 cc/rain.
76.99
0.5028
May 27, 1971
EXB-3
Time
minutes
1
2
3
It
5
6
7
8
9
10
.12
lit
16
18
20
25
30
35
itO .
1*5
50
55
60
65
70
75
80
85
90
95
100
110
.120
J30
DK>
J',0
1 60
JYO
JfiO
1 <>0
,'00
;MO
;-20
:?_;0
piio
250
260
270
p8o
?90
300
Load
ing. H2SO),/g. C
3.87
14.88
5.62
6.36
7.10
7-83
8.57
9-31
10.014
10.78
12.35
13-91
15.57
17-23
18.89
23. Ill
28.20
33-27
38.89
U5.06
51-33
57.96
61*.. in
70.77
77.22
83.76
91.23
98.51
105-79
113. .16
120.53
135-09
lfi9-37
: 6:^.38
177.29
iyi.9!>
;;o6.oii
;?io.f,«
;><. 58
:'Mi.66
;">:.;. oo
r>< />.('.«
PYY . oo
;>«.,. <>:,
P<'6.17
j,o'i . or1
^i3.f.i
:;;o.05
;::'3.05
.Tj'i-9'S
3)12.06
Mean Load.
mg. H2SOi+/g. C
2
1*
6
8
10
12
lit
16
-- 18
20
25
30
35
1*0
»I5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
ll)0
150
160
170
180
.190
200
220
2liO
?60
;-ao
jOQ
320
3liO
Rate
mg. H2SO^/g. C/min.
3-8703
1.9812
0.7925
0.7l)-6^
0.76148
0.7833
0.8109
0.8386
0.8662
0.8938
0.9583
.1.0229
1.0781
1.12142
. 1.1703
1.2072
1. 2l4l40
1.2809
1.3085
1.3362
1.3638
1 . 3822
1.1(007
1.14191
1.^375
DA67
1.14652
1.1471414
l.VfWk
1.1)652
1.U560
1.^375
1 . li099
J . 391)1
J 3638
l .330?
l.?
O.'W^l
O.R017
0.6'OJ
409
-------
i; H A V I M K T H 1 C !' I. <> W K X 1' K K I M !! N T !'.
Hun: 3 >(>-(";
Dry Weigh' : 103.60 ing.
Deflection: -5-90 i::g.
2000 ppra
EXC-1
NO: 0 pp:n
02: 3-5"
H20:
S02:
Carbon:
Time
minutes
3
2
3
)i
5
6
y
8
9
10
12
Hi
16
18
?0
25
30
35
1*0
145
50
55
60
65
70
75
80
t'j
90
0';
.1.CX)
no
.12(1
1 -if)
l'in
!'.)<)
ViO
jyo
IMO
1Q( >
20d
2.10
220
2<0
2UO
2'/>
P-.0
270
,'^0
L>'»U
iOO
Load
me- H2::o)(/g. c
9.27
10.1(2
31.29
12.16
32.93
33.80
Di.67
15.1('i
16.33
37.30
18. H2
20.66
22.39
2U.33
25-97
30.60
35-52
1+0. 61*
l*6.ll*
51. 7!*
57-53
63.51
69.50
75.68
81.76
88.03
oH.2l
100. ^9
106 . r>G
132. 8'i
3.:i-).i3
13.1. 1 H
1 1(2. <.>5
iVl.'l'i
,lf.',.r,l|
jyi'..'1'.j
.!(''.. '17
]<>Y.10
2i .1,1')
23.i.,.>'i
22-\. Ij
2 -U.' . ;i J,
2lfO.S-l
2lj';.,,S
2'ii', . 3..S
1, , . '")
27>\,'7
jy--."-;
^i.-':fi
^'.'is
;M'i.]y
t:
200 CF
Ft:
% HgSOj,.:
Correction:
Date:
1500 ce/min.
75-15
0.1*908
May 28, 1971
Mean Load
mg. HgSO^/g. C
6
8
10
12
Hi
16
38
-, 2.0
25
30
35
l|0
1)5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
l'*0
350
160
iyo
.180
190
?_oo
220
ii'lO
2/,0
280
.
Rate
mg. H2SO^/g. C/min.
7.1i*29
1+.1988
1.1390
0.8687
0.8301
0.8398
0.8591
0.878)f
0.9266
0.97^9
.1.0232
1 . 0?lU
1.100)i
1.1293
1.1583
1.1873
1.1969
1.2162
1.2259
1.2355
1-2355
1.2355
1.2355
1-2355
1.2259
1.2162
1.3-969
1.1680
l.lif«6
1..U97
1.0907
. 1.0610
1.02 =52
().
-------
GRAVIMETRIC FLOW EXPERIMENTS
Run:
Dry Weight:
Deflection:
SO :
Carbon :
159-G
102.26 mg.
-5-93 mg.
2000 ppm
EXA-2
NO:
V
HO:
tf
0 ppm
3-5*
%
200° F
'.V
1500 cc/mln.
79- 44
Correction: 0.5188
Date: June 7, 1971
Time
minutes
1
2
3
>t
5
6
7
. 8
9
10
12
14
16
18
20
25
30
35
ho
45
50
60
70
Ro
VO
100
11,0
120
1.30
I'lO
150
160
170
180
190
200
2.10
' ??0
230
2'c.)
no
260
','/0
?.",o
;> m
300
Load
ng. H2SOl,/g. C
2.64
3-52
3.91
4.20
li.'jO
k.(f)
II.B-J
5.0^
5.28
5.38
5.67
5./r
6.26
6.55
6.75
7-53
8.31
9-00
9.68
10.37
11.05
12 . 52
13.89
.15-45
Jfi.'tf
I,",J|H
19-95
21.51
P3.0H
24.64
26.31
i'7-07
29-73
31 39
33.15
31' 91
36.77
3>"-63
ii0.5»
ii;;.54
hh.'j-*
46//4
4't.H'i
51..24
'>V'>
56.13
Mean Load
ing. HaSOlj./g. C
4
6
8
. 10
' ie
1)1
16
18
20
25
30
35
40
45
50
55
Rate
nig. HgSO^/g. C/min.
0.3071
0.1604
0.1408
0.1418
0.1438
0.1457
0.1486
0.1516
0.1555
0.1633
0.1741
0.1868
0.2005
0.2151
0.2318.
0.2494
411
-------
GRAVIMETRIC FLOW EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
165-G
106.92 mg.
-5-97 mg.
2000 ppm
EXA-3
NO:
02:
HgO:
t:
0 ppm
3-5$
656
200° F
t
1500 cc/min.
2h: 77-85
Correction: 0.5084
Date: June 16, 1971
Time
r.inutes
1
2
3
4
5
6
7
8
9
10
12
14
16
10
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
1 60
170
180
190
POO
?10
2PO
'30
shn
'50
('/>
'(<>
;'r>
> .-)8
^'i?.70
',"j\ . »'.
;'u).4'(
;'i»i'.".o
'.''(<''/>
:''-'J.v'"
P "l.l.-',
P >{. I'l
^05.40
jo i.'iM
:. 03
]..Y'l
Mean Load
mg. HpSOjj/g. C
' ' ' "
2
4
6
8
-'10
12
Ik
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
3.40
150
160
170
180
190
POO
220
2l)0
260
?;*o
300
3?o
Rate
ing. HpSOk/g. C/rain.
4.2088
2.5907
1.6835
1.1785
0.9727
0.8605
0.7669
0-7202
0.7108
0.7295
. 0.7856
0.8230
0.8698
0.9166
0.9540
J. . 0007
1.0382
1.0156
1 1130
1.1504
1.1785
1.2065
1.2252
1.2439
1-2533
1.2626
.1.2813
1.283.3
1.2720
1.2626
1.2439
1.2252
1.1972
1.1691
1.1504
1.1130
1.0382
0.95)10
0.8605
0.766)
0.6640
0 . 563 f>
412
-------
GRAVIMETRIC PLOW EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
166-0
101.36 mg.
-6.09 mg.
2000 ppm
EXA-4
NO:
02:
HgO:
t:
0 ppm
3-5$
6$
200° F
Ft:
Correction:
Date:
1500 co/tnin.
77.20
0.5042
June 21, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
10
12
It
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
I'lO
.100
.1.60
J.YO
.1 HO
1 'X>.
;?oo
21.0
;vo
;>30
P'lO
250
260
270
2MO
2-)0
'(00
Load
ing. H2SO^/g, C
4.o4
5.82
7.20
8.29
9.27
10.26
11.25
12.33
.1,3.32
lit. 31
16.18
18.15
19.93
21.80
23.78
28.12
32.66
37.19
iH. 83
46.47
51.30
61.76
73-01
84.55
96.98
110.00
12P.93
135.06
l4Y.'lO
1 V.i. 83
172.36 . . . .
LS'l . 19
.1 >J'j . Y'l
;K>6.3v
P,l/).'j'3 . ..
226. >'!
23S.Y9
P'i4.0Y
2V-;.B'j
Pfr'.Oli-
069. »3
2YY.'t3
2811.63
291.5'!
2->H.L5
30'i . 66 . ... ...
Mean Load
mg. H2SOij/g. c
2
.4
6
8
' 10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
1.10
120
130
140
150
160
170
180
190
POO
220
240
260
280
300
Rate
mg. HgSO^/g. C/min.
4.0450
2.4862
1.6180
1.1346
1.0359
0.9767
0.9471
0.9373
0.9274
0.9175
0.9077
0.9126
0'.9175
0.9422
0.9570
1.0014
1.0359
1.0754
1.1099
1.1444
1.1691
1.1938
1.2135
1.2332
1.2480
1.2579
1.2727
1.2727
1.262H
1.2579
1.2382
J .2184
1.1938
I.l6)i2
i.J3'i6
1.0951
1 .0162
0.0274
0.828Y
0.7202
0.6215
413
-------
GRAVIMETRIC FLOW EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
167-G
107-14 mg.
-5-99 mg.
2000 ppm
EXA-5
NO:
02:
H20:
t:
0 ppm
3-5$
6$
200°F
t
Correction :
Date:
1500 cc/min.
77-51
0 . 5062
June 23, 1971
Time
ninuteo
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
.100
no
IP'O
1.30
UlO
1^0
160
170
180
1^)0
?00
210
?J.'0
30
J'|0
"jO
'l:i)
'(()
': '< )
')}
sou
Load
inc. HgSOjj/g. C
3-17
4.67
5-69
6.53
7-37
8.12
8.87
9.52
10.17
10.83
12.13
13.44
14.75
16.15
17-55
21.09
24.64 .
28.19
31-83
35-56
39.39
47.23
W-44
64.60
74.30
84.66
95-30
106. 4 o
117.51
128.62
139.54
I.b0.64
161.56
172.58
J83.22
193. 2 L
202.91
212. 'j 3
22L.95
231.10
2S'.'.';/1
PW.iM
P'jY.'jl
f'(,fi.".j
L'lV.OY
;>Y;i.:(...
Mean Load
ing. HgSOjj/g. C
2
4
(>
8
' 10
12
14
16
18
20
25
30
35
ho
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
i4o
150
160
170
180
190
200
220
240
260
2MO
Rate
mg. l^SO^/g. C/min.
2.7067
1.6054
0.9_520
0.7467
0 . 7000
0.6814
0.6720
0.6814
0.6860
0.6907
0.709^-
0.7280
0.7560
0.7840
0.8167
0.8494
0.8867
6.9240
0.9614
0.9894
1.0080
1.0360
1.0500
l.o64o
1.0780
l . 0420
l . 1060
1 . .1 107
1.1107
.1.3014
1 . 0920
1.0780
1.0594
1.0407
1 . 0174
0.9894
0.9334
0.8yi7
0.7840
0.70^4
414
-------
GRAVIMETRIC
FLOW
EXPERIMENTS
Run:
Dry Weight:
Deflection :
S02:
Carbon:
if, 9- a
100.50 ing.
-5.91 n«-
2uOO ppm
]:>:;- 4
NO:
02:
H20:
t:
0 ppm
3f~ ^
)"!'
6%
200° F
Ft:
Correction:
Date:
1500 cc/inin.
78.24
0.51105
June 25, 1971
Time
minutes
1
2
3
l)
5
6
7
8
9
10
12
lit
16
18
20
25
30
35
ho
45
50
60
70
80
90
100
110
120
I'-JO
.11)0
150
IhO
.170
IMG
J'lO
2UO
2.1 n
220
2-iO
2-'.0
2''0
;>r,o
270
,''',(}
','.'l<>
':< )0
Load
m.";. H230i|/(;. C
1+.73
6.17
7.06
ti.or,
8.96
9.95
10.95
11. 9'J-
12.9U
13-93
16.02
18.31
20.50
22.89
25.17
30.95
37. lH
Mt.68
52. Mi
60.80
69.65
88.36
107.96
128.26
11*9.25
169.75
189.75
20H.96
226.97
2l)3.(.rt
2!>Q.oO
275-02
|_ 290.05
30.5 . 08
l.Tt.'H
J,20.''7
j, j,<,. ','.:>.
Vin. 17
V..'.. :2
V l-'l .'..')
W.2'i
;7< I . ' in
.-.7.1"
-.I.IM
)|E 1 ] t\>> t
h>>{.'/t.
Moan Load
rng. HaSOl^/R. C
1)
6
8
10
-' 12
14
3.6
1.8
20
25
30
35
Uo
45
50
55
60
65
.70 .
75
80
85
90
95
100
110
120
130
1.40
150
160
170
180
190
200
2.?0
2'lO
2f,0
2MO
HOO
;HO
;'iO
li .0
VH>
lino
Rate
mg. HjjSO^/g. C/min.
3-l«4l
1. 2'I38
0.9254
0.9552
0.9751
1.0149
1.0348
1.0647
1.0945
1.1741
1.2637
1.3433
1.4229
1.4975
1.5672
1.6418
1.7015
1.7612
1.8109
1.8607
1.8905
1.9204
1.9602
1.9900
2.0100
2.0498
2.0697
2 . 0796
2.0796
2.0697
2.059V
2 . 0398
2.0000
1.9'".C2
l.Ol.Oli
1.7"' 0
l.
-------
G R A V I M K T H I C ]' L 0 W K X P K H I M E NTS
I'uri:
Dr.y WeM'L:
D< riwt.jon:
C02:
Carbon:
1.7"-'!
.Kv'.'.'i nit'.
-5. 'i.l me,.
2000 ppm
EXB-5
NO:
HgO:
C) ppm
3.5$
6*
200° F
]?t: 3-500 I'
$ HgSOj,: 78.4?
Correction: 0.532)4
Date: June 28, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
10
32
3.1)
36
3.8
20
25
30
35
Uo
>45
50
60
70
80
90
100
110
120
HO
1'jO
ISO
'li.U
170
i.'-;o
3 ' '0
2oo
23.0
2.-i '
2 -;(.'
.-.'llO
2M>
i.'i i)
270
2.''d
2' 40
J,t «.)
J, It)
j- );^
> -ll '
Load
mr.. T!?SOb/«. C
U.19
6.33
7.79
8.87
9-9'*
11.01
32.08
3.3.06
13-93
1)4.71
16.56
3.8.61
20.65
22 .<>0
25-23
31.18
37.61
14)4.72
52.51
60.80
69.66
88.56
108.73
329.87
150.lt|
170.01
188.91
206.55
223-79
2'i0.55
2y>.M
27.1.. 0)+
2M . 3 0
2'i',.8i,i
307. f»
-11'".. 00
:2».5i
', ;.-f.O^
;'ii,.(.S
-;-']. is
','1 .in,
-;.,".. |.-i
'.Y'«.< !
'.-'. 1 .»'li
-,--;y.2,;>.
; i -i . .12
.i.".. 87
)K''I .o-j
llU'^.UO
Mean Load
mg. H2SO^/g. C
2
If
6
8
10
12
14
16
18
20
25
30
35
1)0
'45
50
55
60
65
70
75
80
85
90
95
100
1J.O
320
130
lUO
.1.50
160
370
180
wo
200
220
2*10
A ,0
2H<>
',00
^20
.)l|0
-:f'.o
--i»o
InOO
Rate
mg. HgSO^/g. C/min.
^. 38)43
2.7280
1.5680
1.^322
1.0035
0.9353
0.9256
0.9^99
0.98^0
1.0279
I.l₯t8
1.2U22
1.3396
3..U322
1.5101
1.5881
1.6660
1.73^2
1.7927
1.8)463
1.8950
1.9339
1.9729
1-9973
2.0216
2.0)460
2.0703
2.0752
2.0703
2.0557
2.02.16
.V.9B75
1.9)186
l . 90uf>
3.H706
1.8.1YO
3..7050
l-'/C-'V-i
i.'i m.
3 .271--!
1..I2())J
D.')7'H
o.^v/o
0.7210
o.r.oaq
0.52bl
416
-------
r, K A V I M K T li T C V T, 0 W V X I' K R T M K N T I',
Run:
Dry Weight:
Deflection:
S02:
Carton:
171-C!
101.80 nig.
-6.22 mg.
2000 ppm
EXA-4
Time
minutes
1
2
3
14
5
6
I
8
9
.10
X?
3.4
16
18
20
25
30
35
1+0
U5
50
60
70
80
90
100
330
120
1 '.()
1.4 0
I'/'
K.d
:iY''>
.U'f'
]nO
21 >'')
2JO
22"
2-:o
24 o
2',...
2.'0
270
2.' 0
2' -C>
inn
Load
mg. HgSO^/g. C
5-50
7-56
9.014
30.32
11.. 20
12. 2H
13-26
lH.35
1^-93
l'j.82
37-°'.)
3.8.76
20.04
21.U1
22.99
26.82
31.04
35-66
1*0.37
U5.28
50.29
60.81
71.51
82.91
9'i-79
.106.88
31 9- 35
131.93
l.'i'i.Ol
.V/-.80
l(>7.r;<'i
17H . * .rt
380.30
.v>',).:i2
2i'.'i.Wi
23.8. liy
227.70
236.7!)
24S.68
2[.;'i . .«
2i..-!.'-!7
270.02
2V.J.2M
2J-.4.7.7
?>').{'('
;?»...*>;
J2'
U2C
t:
H20:
0 ppm
3.536
e*
200° F
*t:
1500 cc/niJn.
77.04
Correction: 0.5031
Date: June 29, 1971
Mean Ixsad
mg. HgSO^/g. C
2
It
6
8
10
"' 32
lit
16
18
20
25
30
35
ItO
it5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
3/.0
170
18'0
190
200
220
240
260
280
300
Rate
mg. HgSO^/g. C/min.
6.5815
3-6337
2.4558
1.5226
1.2083
0.9921
0.874.3
0.7«59
0.7466
0.7367
0.7957
0.8^46
0.9037
0.9627
0.9921
1.0314
1.0609
1.0904
1.1198
1.1395
1.1591
1.1788
1.3886
1.2083
.1.23.81
3.. 2279
1.2377
1.2475
.1.2 ',77
.1.21 H.I
J.lHHi,
1 ..l'/)l
3 . 1297
3 .1002
1.0609
.1.02.16
0.9528
0.8743
0.7859
0.6876
0 . 5094
417
-------
r; R A v :i M !; 'i1 K i c
LOW K X ]' K K 1 M E N T !i
Him:
Pry Welch t:
Deflection :
S02:
Carbon:
172- G
100. ll* m;'..
-6.13 mg.
2000 ppm
EXC-2
NO:
02:
H20
t:
0 ppm
200° F
Ft: 1500 cc'/rain.
% H2SOi+: 76.89
Correction: 0.5021
Date: July 8, 1971
Time
minutes
\
2
>>
1(
5
(',
7.
B
9
1.0
.12
111
16
18
20
25
30
35
1(0
'45
50
60
70
HO
90
100
110
.120
.1 «)
ll|()
ISO
-|.'.Q
17U
I.'"-)
I'/O
;_'-.o
..' 10
.'.w
?.'-.<>
^«
.?'.o
' 'i "
,-yo
':' '-ll
.' "'
',()!)
Load
me.. H2SOj,/c;. C
i JlO
5 19
(>. -iO
7.S')
H . vy
).2'i
K). 19
1i).')M
11. HM
' 12. (',8
I'l-.'iH
16 . 1.7
17-97
19.87 .
21.77
26.86
32.15
37.85
1*3.714
50.33
57-02
71 . 10
«fj.f,8
.10^.26
.ll'i.'M
l',f,.K.I.
J5',.7'
170. ','
j. '-;,,. N'I
2ul .22
<-'!'.. 1.0
iNo. ;:
2Mi.)|,,
2'>-.2i4
271.52
2 U..-M
2- "1. 7s.'
-iill .'.-.
i.'.ir.
^ . i -.
MI .«.';
''- '.'>.?
.' '.11
'.....' u
.1 ; . ' .' i
V(".i .'>
418
Moan Load
me- l^SO^/g. C
2
l|
6
.- 8
10
12
111
ir,
18
20
25
30
35
ko
1+5
50
55
60
65
70
75
80
85
90
.95
.100
.1JO
.120
1 J,0
1'40
150
160
170
.1.80
190
200
220
2UO
2.'0
280
WO
#0
s'.o
Vfl
Rate
mg. HgSOjj./g. C/min.
2.9^59
]..877'i
1.2l|«3
0.9087
0.8238
0.0.1H9
O.H'MH
0.87.-S8
0.9*7
0.9J87
1.0136
1.0/85
l.lUSlf
1.2033
1.2582
1.3132
1.3581
1.1*030
1.14-1*30
1.1*779
1.5179
1.5W
1.5728
1.5978
.1 .6177
:i .6 <77
.1 .u;a
l.''77Y
)..^Hr!d
l.C>777
l.f.f.77
I.c,'i77
1.6227
1.5978
1.5678
1.5279
l.'*530
1. 368.1.
1.2682
J . 1.68'i
J .oi>8s
0.
-------
GRAVIMETRIC FLOW EXPERIMENTS
Run:
Dry Weight:
Deflection :
S02:
Carbon:
175-G
102. 56 ing.
-6.16 ing.
2000 ppra
EXC-3
NO:
02:
H20:
t:
0 ppm
3.5%
6.0$
200° F
t
1500 cc/min.
73-58
Correction: 0.1+980
Date: July 16, 1971
Time
inj nutos
1
2
3
k
5
6
7
8-
9
10
12
lit
16
18
20
25
30
35
1+0
U5
50
60
70
80
90
100
110
120
130
l!|0
150
160
170
180
300
200
230
<«(>
2 '',()
2'iO
2'.<0
?V>0
270
2.<<>
2')0
3(10
Load
ing. HgSOli/K. C
6.3^
8.29
9-5<>
10.l|\
11.31 -
12.09
12.77
13.W
1H.1.1+
1.1+.72
16.19
17.55
19.01
20. 1*8
22.01+
26.23
30.91
. 36.08
lU.Mt '
1*7.19
53-33
66.50
80. 5'+
95- H6
1.10.18 .
125-39
lit 1.38
157.37
172.87
.188.09
201.93
21.lt. 90
228 . 16
21(1.22
253- Jil
265. Ill
276. <0
.2H7.(i'i
2', ,'7. 00
'.U) . IK'I
.', I'l .'i)|
32 x.('.r;
^1.71.
i -i'-).ii.i
',iir,.;,;!
Hr< '<.')'(
Mean Load
mg. HgSOl^/g. C
2
1+
6
8
10
-, :i2
ii*
16
18
20
25
30
35
1+0
't5
50
55
60
65
70
75
80
85
90
95
1.00
110
120
130
1^0
150
160
170
180
190
200
220
21+0
260
280
300
320
i'K)
Rate
mg. HgSOij/g. C/min.
8.239],
5 1677
3.120.1
1.7'i53-
0.8970
0.7110
0.6533
0.6728
0.7215
0.7605
0.8678
0.9555
1.0238
1.1018
1.1603
1.21.88
1.2676
1.3066
1-3358
1.37W
i.i+oin
1A333
1.1(528
lA?23
I.li91.8
1.5113
.1.5308
1.5503
1.5601
1.5601
1-5503
1.5308
1.5113
1.U821
l.Ul+31
l.l+oUi
1 . 3066
1.2188
1.1.1|08
1.0628
0.0653
0.8678
0.760',",
419
-------
APPENDIX A-15-2
SURFACE AREA AND PORE VOLUME DISTRIBUTION
OF SOLVENT EXTRACTED CARBON
Surface area and pore volume distribution measurements were
made by means of nitrogen isotherms on the Englehard Isorpta,
Englehard Industries, Inc., Newark, New Jersey. The surface
area was calculated from the BET equation12* and the pore
volume distribution with a computer program we have using the
Roberts13 method of pore determination. In the tables given
in this section, REL P is relative pressure and VOLUME is
volume adsorbed of nitrogen in cc./g. C. Other designations
are S = surface area in m2/g. C; C = the BET constant, and
R = the correlation coefficient. PORE RADIUS is the range
of pore size in A; VOL is the volume in cc./g. C in that
range; and CUMV is the cumulative volume to that point.
*References are listed in Bibliography, Section 8, in
Volume I.
420
-------
SAMPLE: EXA-1
RFL P
v/OLUME
U. 1423
o. i 7a2
0.2141
0. 3219
0.4296
0.5374
0.6452
0. 7529
O.t,607
0.9685
S 193.
C -34
R 0.9980
0.09.13
0.0990
0.1015
0.1078
0.1135
0. 1182
0.1226
0.1260
0.1318
0.1389
7
.257
PORE RADIUS
VOL
CUMy/
1000.
500.
400.
300.
200.
150.
100.
90.
dO.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
U.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0012
0.0006
O.OOC9
0.0016
0.00 I1* "
0.0027
0.0009
0.0011
O.OC13
0.0017
0.0021
0.0015
0.0018
0.0022
0.0029
0.0043
0.0063
0.0041
0.0055
0.0070
0.0076
A. 0.0114
0.0012
0.0018
0.0026
0.0042
U.OObY
O.OOt'4
0.0093
0.0103
0.0116
0.0133
0 . 0 lt> 7
0.0172
0.0191
0.0213
0.0242
0.0285
0.0353
0.0394
0.0449
0.0519
0.05vl>
0.0700
421
-------
SAMPLE: EXA-2
REL P
VOLUME
PORE
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
0.1488
0.1865
0.2243
0.3375
0.4508
0.5641
0.6773
0.7906
0.9039
0.9869
S 167.7
C -28.
R 0.9991
RADIUS
500.
400.
300.
200.
150.
100. - -
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0856-
0.0878
0.0900
0.0966
0.1028
0.1003
0.1133
0.1180
0.1234
0.1287 .-
132
VOL
0.0009
0.0004
0.0007
0.0013
0.0012
0.0023
0.0008
0.0010
0.0012
0.0016
0.0023
--0.0015
0.0019
0.0024
... .. . 0.003i
0.0048
0.0078
0.0047
0.0059
0.0070
0.0077
0.0077
CUMV
0.0009
0.0013
0.-0020
0.0032
0.0045
0.0068 -
0.0076
0.0085
0.0097
0.0113
0.0136
0.0151
0.0170
0.0195
0.0227
0.0275
0.0353
0.0400
0.0459
0.0529
0.0606 " ' '
0.0683
422
-------
SAMPLE: EXA-3
REL P
VOLUME
PORE
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
lb.
16.
14.
12.
0.1488
0. 1865
0.2243
0*3375
0.4508
0.5641
0.6773
0.7906
0.9039
0.9869
S 650.9
C -20.
R 0.9983
RADIUS
500.
400.
300.
200.
150.
100. -
90.
80.
70.-
60.
50.
_._-_... 45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.3620
0.3684
0.3731
0.3850
0 . 3 94 8
O.'»027
0.4096
0.4161
0.4231
0.4296--
340
VOL
0.0010
0.0005
0.0008
0.0016
0.0015
0.0029 -
0.0010
0.0012
- 0.0016 - -
0.0021
0.0030
0.0021
0.0026
0.0034
0.0045 -
0.0066
O.Olll
-- 0.0071
0.0094
0.0120
0.0151
0.0210
CUMV
0.0010
0.0015
0.0023
0.0039
0.0054
0.0084-
0.0093
0.0106
0.0121
0.0142
0.0173
-0.0194
0.0220
0.0254
-0.0299
0.0365
0.0476
0.0547
0.0641
0.0761 "
-0.0912
0. 1122
423
-------
REL P
SAMPLE: EXA- 5
VOLUME
0. 1428
0.1791
C.2153
0.3241
0.4328
0.5416
0.6504
0.7591
0.8679
0.9766
0.3382
0.3430
0.3478
0.3588
0.3683
0.3759
0.3831
0.3898
0.3975
0.4093
S 620.8
C -22.416
R 0.9985
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0026
O.OG10
0.0015
0.0026
0.0023.
0.0041
0.0013
0.0015
0.0019
0.0025
0.0035
0.0024
0.0029
0.0036
0.0048
0.0069
o.oion
0.0066
0.0092
0.0117
0.0133 -
0.0201
0.0026
0.0037
0.0052
0.0079
0.0102
0.0143
0.0155
0.0171
0.0190
0.0215
0.0250
0.0274
0.030H
0.0339
0.0387
0.0456
0.0564
0.0630
0.0722
0.0840
0.09'M
0. 1174
424
-------
SAMPLE: EXB-3
REL P
VOLUME
0.1426
0. 1788
0.2151
0.3237
0.4323
0.5409
0.6495
0.7581
0.8667
0.9753
S 667.
C -22
R 0.9986
0.3636
0.3690
0.3734
0.3855
0.3956
0.4039
0.4115
0.4184
0.4257
0.4350
5
.456
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0015
0.0007
0.0010
0.0019
0.0018
0.0034-
0.0011
0.0014
0.0018
0.0024
0.0034
0.0023
0.0029
0.0038
0.0051
0.0074
0.0119
0.0073
0.0097
0.0125
0.0156
0.0187 -
0.0015
0.0022
0.0032
0.0051
0.0069
0.0104
0.0115
0.0129
0.0146
0.0 1 70
0.0204
0.0227
0.0256
0.0294
0.0345
0.0419
0.0538
0.0611
0.0708
0.0833
0.0990
0.1176
425
-------
SAMPLE: EXB-4
REL P
0.9741
VOLUME
0.1425
0.1786
0.21^8
0.3232
0.4317
0.5402
0.6487
0.7571
0.8656
0.3720
0.3772
0.3816
0.3931
0.4023
0.4100
0.4167
0.4237
0.4309
0.4407
S 680.1
C -22.182
R 0.9986
PORE RADIUS
VCL
CUMV
1000.
500.
400.
30U.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40. .
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0021
0.0008
0.0013
0.0022"
0.0020 '
O.OC35
O.OOll'
0.0014
0.0013
0.0024
0.0034
0.0023
0.0030
0.0039
0.00.49
0.0063
0.0106
0.0068
0.0089
0.0115
0.0148
--0.0189
0.0021
0.0030
0.0042
0.0064
0.0084
0.0119
0.0130
0.0144
0.0162
0 . 0 1 b 5
0.0219
0.0242
0.0272
0.0310
0.0360
0.0423
0.0529
0.0597
0.06U6
0.0800
0.0948
0.1137
426
-------
SAMPLE: EXB-5
REL P
VOLUME
.. -
PORE
1000.
500.
400,
300.
200,
150*
100.
90.
80.
-- - - \f *^ w
70.
60.
50»
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
0.1484 ...
0.1860
0.2237
0.3366
0.4496
0.5626
0.6755
0.7885
0.9015
0.9994 ....
S -73K4
C -19.
R 0.9983
RADIUS
500.
400.
300.
200.
150.
100*
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
o.4ioa
0.4169
0.4213
0.4334_ __,_.
0.4439
0.4530
0.4 60! ,_.
0.4679
0.4756
0.4842
859
VOL
0.0011
0.0005
0.0009_.^...
0.0017
0.0017
... 0.0032... ..
0.0011
0.0013
0.0017 .
0.0023
0.0034
u O.OQ24
0.0030
0.0038
0.0051 . ..
0.00/3
0.0128
0.0080 .
0.0102
0.0125
0.0148
0.0188
CUMV
0.0011
0.0017
fl.0026
0.0043
0.0059
._ 0.0091
0.0102
0.0115
0.01 H
0.0156
0.0190
o.opn
0.0243
0.0282
_ 0.0332
0.0405
0.0533
_ . 0.0613
0.0714
0.0839
0.0988
0.1175
427
-------
SAMPLE: EXC-1
REL P
VOLUME
0. 1426
0. 1788
0.2151
0.3237
0.4323
0.5409
0.6495
0.7581
0.8667
0.9753
S 628.
C -22
R 0.9985
0.3442
0.3489
0.3531
0.3634
0.3722
0.3805
0.3873
0.3937
0.4007
0.4132
0
.024
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0040
0.0014
0.0020
0.0031
0.0025
0.0041
0.0012
0.0015
0.0018.
0.0023
0.0032
0.0021
0.0027
0.0034
0.0045
0.0065
0.0115
0.0073
0.0086
0.0104
0.0127
0.0174 '
0.0040
0.0054
0.0074
0.0105
0.0130
0.0171
0.0 l»3
0.0197
0.021r>
0.0238
0.0270
0.0291
0.0318
0.0353
0.0398
0.0463
0.0578
0.0651
0.0737
0.0841
0.0963
O.U41
428
-------
SAMPLE: EXC-2
REL P
VOLUME
R
736.8
-20
0.9982
PORE RADIUS
1000.
500.
400.
300.
200.
150.
.100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200*.
150.
100.
-90.
80.
70.
60 »
50.
45.
- 40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.4102
0.4172
0.4232
0.4348
0.4459 ._
0.4553
0.4624
0.4688
0.4768
0.4838
t
304 ..
VOL
0.0003
0.0004
0.0007
0.0016-
0.0017 '
0.0035
0.0012-
_ ,. ._ - -^0 ^ ^f %^*«r ^ff^-f-m^,
0.0015
0.0019
0.0024
0.0034
0.0021
0*0026
0.0033
0.0044
. .-0.0068.-.-
0.0132
0.0086
0.0109 ..
0.0125
0.0133
- 0.0262 .-
CUMV
._.._ 0.0003
0.0007
0.0014
0.0030
0.0047
0.0082
0.0094
0.0109
0.0127
0.0151
0.0185
0.0206
0.0232
0.0266
0.0310
0.0378
0.0510
0.0596
_. 0.0705
0.0831
0.0964
0.1226
429
-------
SAMPLE: EXC-3
REL P
0.1478
0.1853
0.2228
0.3353
0.4478
0.5604
0.6729
0.7854
0.8979
0.9880
VOLUME
0.4228
0.4291
0.4338
0.4453
0.4553
0.4634
0.4707
0.4780
0.4857
0.4925
S 752.8
C -19.881
R 0.9983
PORE RADIUS
VOL
1000..
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
. 500.
400.
300.
-200*.
150.
100.
-. .... . 90.
80.
70.
... 60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
--- 10.
. ... -0.0006
0.0004
0.0007
0.0015
0.0016
0.0032
0.0011
0.0014
0.0018
0.0024
0.0034
0.0024
- ~~ 0.0030-
0.0039
0.0050
, 0.0070
0.0113
0.0071
- 0.0096
0.0119
0.0142
-.._ 0.0202-
CUMV
0.0006..
0.0010
0.0017
-O..0032-
0.0048
0.0079
0.0090
0.0104
0.0121
0.0145.
0.0179
0.0203
-0.0233-
0.0272
0.0322
0.0391
0.0504
0.0575
0.0671
0.0790
0.0933
0.1135
430
-------
SAMPLE: EXD-1
REL- P
0.1860
0.2237
0.3366
0.4496
0.5626
0.6755
0.7885
0.9015
0.9919
VOLUME.
0.0769
0.0792
0.0818
0.0896
0.0964
0.1019
0.1072
0.1121
0.1176
0.1236
S 158.4
C-. -37.043
R 0.9995
PORF RADIUS
VOL
CUMV
* v >^ v* »
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
400.
300.
200.
150.
100.
90.
80.
70.
60. -.-..
50.
45.
40.
35.
30.
25. .,
20.
18.
16.
14.
12.
10.
0.0009
0.0004
0.0007
0.0013
0.0012
0.0024
0.0008
0.0010
0.0012
0.0017
0.0024
0.0016
o_no ?o
\J % \J \J *-~ v
0.0026
0.0035
0.005 1
Vr
-------
SAMPLE EXH-1
REL P
VOLUME-
PORE
1000.
500.
400.
300.
200.
150.
100.
90.
BO.
70.
60.
50.
45.
40.
35.
30.
25.
20.
IB.
16.
14.
12.
0.1484
0. 1860
0.2237
0.3366
0.4496
0.5626
0.6755
0.7H85
0.9015
0.9919
S 721.
C -19
R 0.9984
RADIUS
500.--
400.
300.
..... 200.
150.
100.
- 90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.4065
0.4106
0.4156
0.4278
0.4383 -
0.4471
0.4544
0.4619
0.4696
0.4781
7
.848 - -~- -----
vot
-0.0014
0.0006
0.0010
0.0018
0.0017
0.0032
O.OOU
0.0013
0.0017
0.0023
0.0034
0.0025
0.0031
0.0040
0.0049
0.0069
0.0121
0.0078
0.0102
0.0127
0.0150
0.0192
CUMV
0.0014
0.0021
0.0030
0*0048
0.0065
0.0097
0.0108
0.0121
0.0138
0162
0196
0220
0.0251-
0.0291
0.0340
0.0409
0.0531
0.0608
0.0711
0.0837
0.0987
0.1179
432
-------
SAMPLE: EXN-1
REL P VOLUME
0. 1426
0.1788
0.2151
0.3237
0.4321
0.5409
0.6495
0.7581
0.8667
0.9753
0.1570
0.1603
0.1638
0.1721
0.1791
0.1850
0.1900
0.1944
0.1996
0.2074
S 302.4
C -26.573
R. 0.9988
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0015
0.0007
0.00 10
0.0017
0.0016 .
0.0028
0.0009
0.0011
0.0013
0.0017
0.0024
0.0016
0.0018
0.0023
0.0031
0.0049
0.0083
0.0052
0.0068
0.00 86
0.0103 -
0.0148
0.0015
0.0022
0.0032
0.0049
0.0065
0.0093
0.0102
0.0112
0.0126
0.0143
0.0167
0.0182
0.0201
0.0224
0.0255
0.0304
0.0388
0.0440
0.0508
0.0594
0.0697
0.0844
433
-------
SAMPLE: EXV-1
REL P
VOLUME
0.1428
0.1769
0.2149
0.3231
.0.4313
0.5395
0.5477
0.7559
0.&641
0.9722
S 667.4
C- -22.
R 0.9985
0.3628
0.3636 .
0.3733
0.3851
0.3950
0.4031
0.4103
0 . 4 1 6.8
0.4242
0.4350
«
544
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500. '
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
Id.
16.
14.
12.
10.
0.0022 .
0.00.09
C.0014
0.0024
0.0022-
0.0040
0.0012
0.0015
0.0019
0.0025
0.0034
0.0023
0.002H
0.0035
O.C047
O.OOfO
0.0115
0.0071
0.0096
0.0123
0.0149 '
. 0.0204
. 0.0022
0.0031
0.0045
0.0070
0.0092
0.0131
- 0.0144
0.0159
0.0178
0.0203
C.0237
0.0260
0.0238
0.0323
0.0369
0.0439
0.0554
0.0625
0.0721
0.0844
0.0994
0.1198
434
-------
APPENDIX A-16
EXPERIMENTAL RESULTS OF BENCH SCALE RECYCLE
TESTS - SOLVENT EXTRACTION VERSUS HYDROGEN TREATMENT
1. S02 Sorption Results from 1" Diameter Fixed Bed 436
for (NH4)2S Extracted and H2S Generation
Carbon Samples
2. S02 Sorption Results from Differential Rate 448
Apparatus for (NH4)2S Extracted and H2S
Generation Carbon Samples
3. Sulfur Generation from 1" Diameter Fixed Bed for 453
(NH4>2S Extracted and H2S Generation Carbon
Samples
4. (NH4>2S Extraction Experimental Results 462
5. Pore Volume Distribution Runs for (NH4>2S 468
Extracted and H2S Generation Samples after
Sixth Cycle
435
-------
APPENDIX A-16-1
S02 SORPTION RESULTS FROM 1" DIAMETER FIXED BED
FOR (NH4)oS EXTRACTED AND H2S GENERATION
CARBON SAMPLES
S02 SORPTION RATE
8 31 71
RXT-6-1A
JENPFRATURE =_ 2p8.00QOOO_F
SPACC VELOCITY « 0.299939E 0~4
INLET S02 MOLE FRACTION (DRY) =
/HR
0.002760
INLET H20 MOLE FRACTION «__ _.Q.0.9997.8._ .
INLET OXYGEN HOLE FRACTION = 0.035403
INLET C02 MOLE FRACTION = 0.0
INLET NO KOLE FRAt.II.ON = __ 0.000149
INLET INERT GAS MOLE FRACTION = 6.861992
INLET CARBON WEIGHT = 40.000000 GMS
J.OTAL..GAS. J.COW _= ._7.0.61549_5.CFH
(WET) =
0.0024H4
TIME
MOLE FRACTION.S02.
H2S04 LOADING
CMS ACID/GM C
RATE OF H2S04 SORPTION
GMS ACID/GM C-MIN
0. .
30.
60.
90.
120.
150.
. 180. _ .
210.
240.
_..260. . ._
0. M!>000t-0.*
0.315000E-03
0.396000E-03
._ 0..450000E.-03.
0.660000E-03
0.660000E-03
0.600000E-03 _
0.750QOOE-03
0.920000E-03
0.900000E-03
O.u
0.241539E-01
0.478977E-01
0.709748E-01
0.927576E-01
0.113503E 00
0.134545E 00
0.155143E 00
0.174160E 00
...0.186343E. 00
O.U
0.805129E-03
0.777798E-03
0.760674E-03
0.691522t-03
o.egisi'ZE-oj
0.711279E-OJ
0.661885E-03
0.605905E-03
0.612491E-03
AVERAGE RATE OF S02 SORPTION
0.705465E-03
436
-------
S02 SORPTION RATE
8 31 71
RXT-6-2A
TEMPERATURE = 209.000000 F _
"SPACE VELOCITY = 0.299961E 04"/HR ~
INLET S02 MULE FRACTION (DRY) = 0.002760
INLET H20 MOLE FRACTION * 0.100021
INLET OXYGtN MOLE TRACTION = 0.035045
INLET C02 MOLF FRACTION = 0.0
INLET NO HOLE FRACTICN = 0.000)50
INLET INEK1 GAS MOLE FRACTION = 0.862302
INLET CARPON WEIGHT = 29.899994 GMS
TOTAL GAS FLOW = 5.278689 SCFH
(W6T) =
0.002484
TIME
0
30
60
?.P
120
150.
MOLE FRACTION S02
H2S04 LOADING
GMS ACID/GM C
RATE OF II2S04 SORPTIC.N
GMS ACID/GM C-I-'1N
0.150000E-03
0.150000E--03
0.510000E-03
0.690000E-03
"0.102000E-0?""
0.100500E-02
0.108000E-02
0.120000E-02
0.0
0.257a'tf»E-01
0.497908E-01
0.711296E-01
0.699^030-01
0. 107213E 00
0.124180E 00
0.140185E 00
0.0
0.859484E-03
0.740934E-03
0.681660E-03.
f\ K i "\f\ n i» i~ ^ "»
Wft^i£.'^"w V_*
0.57/929E-03
0.55J231t-03
0.513715E-03
210
AVERAGE,RATE OF S02 SORPTION =
0.642B48E-03
437
-------
S02 SORPTtON RATE
8 31 71
RXT-6-3A
TEMPERATURE = 199.000000 F _
SPACE Vl:i.OCitY * 0.299982E O'l /HR
INLET S02 HOLE FRACTION (DRY) = 0.002780
iiJNLCT H20 MOLE FRACTIQM =. . 0.100036
INLET OXYGEN MOLE FRACTION = 0.034975
INLCT C02 MOLE FRACTION = 0.0
INLIT NO fOLE FRACTIUN = 0.000150
INLET INERl GAS MOLE FRACTION = 0.862338
INLUT CARBON WEIGHT = 30. 11999!> CMS
TUTAL GAS FLOW = 5.3180.99 SCFH _ _
(WET)
0.002502
TIME
MOLE FRACTIOM S02
H2S04 LOADING
GMS ACID/GM C
RATE OF H2SO't SORPTIO^
CMS AC10/GM C-I-'.IN
_ -. 0. ...,.
30.
60.
90.
, 120.
150.
. .lap, ..
210.
240.
0.270000E-03
0.270000E-03
0.420000E-03
0.585000E-03
«,. 780nnoe-0*
0.1035006-02
0.102000E-02
0.916000E-03
0.885000E-03
0.0
0. 2^79796-01
O.A88546E-01
0.7U557E-01
0.920782E-01
0..110576E 00
0.127892E 00
0.145794E 00
0.164363E PO
0.0
0.82659BC-03
0.777199E-03
0.722862E 03
0.65B644e-03
&.574667E-03
0.579607E-03
0.613856E--03
0.624065t-03
AVERAGE RATE OF S02 SORPTION =
0.672186E-03
438
-------
S02 SORPTtON RATE
8 31 71
RXT-6-4A
TEMPERATURE =_ 204.000000 F _
SPACE VELOCITY = 0.299933E 04 "/MR
INLET S02 MOLE FRACTION (DRY) = 0.002780
INLET H20 MOLE FRACTION = 0.100043
INLET OXYGEN MOLE FRACTION = 0.034948
INLET C02 MOLE FRACTION = 0.0
INLET NO fOLE FRACTION = 0.000150
INLET INERT GAS MOLE FRACTION ' =" 0.862364
INLET CARBON WEIGHT = 29.500000 GMS
TOTAL GAS FLOW = 5.207779 SCFH
(WET)
0.002502
TIME MOLE FRACTION S02
0. _ 0.120000E-03
30. 0.120000E-03
60. 0.570000E-03
90. _ 0.750000E-03
120. 0.764000F-03
150. 0.930000E-03
180. 0.1Q3500E-02
210. 0.120800E-02
240. 0.120800E-02
270. 0.1275006-02
290. 0.135000E-02
AVERAGE RATE OF S02 SORPTION =
H2S04 LOADING
GMS ACIO/GM C
0.0
0.262754E-01
0.503282E-01
_0.712694E-P1
0.912524E-01
0.110346E 00
0.128102E 00
0.144485E 00
0.160013E 00
0.175210E 00
0.184874E 00
0.616974E-03
RATE OF H2S04 SORP1ION
GMS ACIO/GM C-MIN
0.0
0.875846E-03
0.727676E-03
C.668408t-03
0.663799E-03
0.517605E-03
0.517605E-03
C.495544E-03
0.470849E-03
439
-------
S02 SORPTION RATE
8 31 71
RXT-6-5A
TEMPERATURE = 206.000000 F
SPACE VELOCITY = 0.299917E 04 /HR
INLET S02 MOLE FRACTION (DRY) « 0.002780
INLET 1120. MOLE FRACTION. = Q.*_LQ.0.0.26_.
INLET OXYGEN MOLE FRACTION = 0.035019
INLET C02 MOLE FRACTION = 0.0
1NLLT NO MOLE FRACTION =. O.OOOIVJ.
INLET INERT GAS MOLE FRACTION = 0.862311
INLET CARBON WEIGHT - 29.279999 CMS
.TOTAL GA.S . FLOW = 5..168670_._$.CJH _
0.002502
TIME . __ MOLF FRACTION S02
H2SO't LOADING
CMS ACIO/GM C
RATE OF H2SOA
GMS AC1U/GM C-HI'N
0.
30.
60.
90,
120.
IbO.
210.
240.
270.
300.
320.
0.270000E-03
0.270000E-03
0.720000E-03
D.87.0000E.-Q3-
0.107000E-02
0.105000E-02
Q..1.0.3.5 0.0 E-Q2_
0.117000E-02
0.135000E-02
0..1A2500E-02.
0.150000E-02
0.150000E-02
0.0
0.247928E-01
O.A73632E-01
0.669702E-01
0.0
0.82642BH-03
0.678264E-03
0.102332E 00
.0_«JL19A94E_P.O..
0.136064E 00
0.151078E 00
00
00
0.186275E 00
0*^7'>'»CCH C3»
0.569610E-03
...0 ..5_7.ft,549E.-_0_3_..
0.530099E-03
.Q,44614_OE-03..
6.42l445t-03
0.421445E-03
AVERAGE RATE OF 502 SORPTION
0.563127E-03
440
-------
S02 SORPTION RATE
8 31 71
RXT-6-6A
_TGMPERATURE_ = 199.000000 F __
SPACE VELOC ITY "~= 6729862 1 FT 04 ~/ll~R
INLET S02 MOLE FRACTION (DRY) = 0.002700
INLET H20 MOLE FRACTION = 0.100015
"INLET OXYGEN MOLE FRACTION = 0.034935
INLET C02 MOLE FRACTION = 0.0
INLET NO MOLE FRACTION = 0.000150
"INLET INERT GAS MOLE FRACTION" =" 0'. 862405
INLET CARBON WEIGHT = 28.500000 GMS
TOTAL GAS FLUW = 5.009249 SCFH
UET) =
0.00243U
TIME
MOLE FRACTION S02
H2S04 LOADING
GMS ACID/GM C
RATE OF H2S04
CMS ACID/GM C-MIN
0.
30.
60.
90.
120.
150.
180-
210.
240.
270.
280.
0.0
0.0
0.390000E-03
0.780000E-03
0.855000E-03
0.930000E-03
0.108000E-02
0.121500E-02
0.118500E-02
0.12'4500E-02
0.129000E-02
0.0
0.265547E-01
0.5H916E-01
0.719927E-01
0.905072E-01
0.108284E 00
0.124954E 00
0.1'i0223E 00
0.154976E 00
0.169581E 00
0.174277E 00
U.O
0.88&157I>03
0.757301E-03
0.629445E-03
0.604857E-03
0.580270E-03
0.531094C-03
0.4K6tt3ot-ui
0.496671E-03
0.477001c-03
0.462248E-03
AVERAGE RATE OF S02 SORPTION =
0.600290E-03
441
-------
S02 SORPTION RATE
8 31 71
RXT-7-1A
^TEMPERATURE = 20.6.000000 £ ..
SPACE VELOCITY = 0.299977E 04 /HR
: INLET S02 MOLE FRACTION (DRY) = 0.002740
L INLET H20 MOLE FRACTION ~ 0.099965_
INLET OXYGEN MOLE FRACTION = 6.035398
INLtT C02 MOLE FRACTION a 0.0
.. INLtT NO MOLE FRACTION = 0.000149
INLET INERT GAS MOLE FRACTION = 0.862024
: INLET CARBON WEIGHT = 40.000000 GMS
,_ryiAL GAS_rLOw = 7.062449 S.CFH :_
(WET>
0.002466
TIME
MOLE FRACTION S02
H2S04 LOADING
GMS ACID/GM C
RATE OF H2S04 SORPTION
GXS ACIO/GN C-MIN'
.0.150000C 03
0.150000E-03
0.210000E-03
0.300000E-03
0.330000E-03
0.345000fc-03
0.570000E-03
0.600000E-03
0.750000C-03
0.0
0.255899E-01
0.508834E-01
0.754359E-01
0.993956C-01
0.123133!: 00
0.145685E 00
0.166977E 00
0.183979E 00
0.0
0.852998E-03
0.8:j3237E-03
0.803596E-03
0.79Jl7l6t-03 """
U. /bH/Yt-t-03
0.714674E-03
0.704793E-03
0.655392E-03
:!: AVERAGE RATE OF S02 SORPTION =
0.770802E-03
442
-------
S02 SORPTION RATE
8 31 71
RXT-7-2A
.TEMPERATURE = 203.000000 F
SPACE VELOCITY" = ~r~ b.299962'E~ "oV/HR ~
INLET SU2 MOLE FRACTION (DRY) = 0.002760
.INLET H20 HOLE FRACTION = 0.099964
INLtT OXYGLN MOLE FRACTION = 0.034952
INLET C02 MOLE FRACTION = 0.0
INLET NO KOLE FRACTION = 0.000150
INLET INER1 GAS MOLE FRACTION = 0.862't!>2
INLET CARBON WEIGHT = 32.409988 GMS
TOTAL GAS FLOW = 5.722059 SCFH
(WET) =
O.C02't84
J I ME
0.
30.
60.
90.
120.
150.
180.
210.
240.
270.
300.
330.
360.
390.
420.
A 50.
480.
4B5.
'ERAG
MOLE FRACTION S02
0.138000E-02
0.138000E-02
0.158500E-02
'.'. 0.163500E-02
0.174000E-02
0.186000E-02
0. 180000E-02
0.16650QE-02
0.162000E-02
0.166000E-02
0.177000E-02
0.166500E-02
0.165000E-02
0.180000E-02
0.186000E-02
0.198000E-02
0.204000E-02
0.202000E-02
E~R ATF"OF '1'02~ SORPT fON
H2SOA LOADING RATE OF H2SOA SORPTION
GMS AC1D/GM C GKS AC ID/ CM C-M1N
0.0 0.0
0.136341E-01 0.454471E-03
0.2625b6E-01 0. 3869!>9t-03
0.376173E-01 _ 0. 370492E-03
0.482134E-01 0. 33591 3t-03
0.576980E-01 0. 296394F-03
0.660062E-OI 0. 31ol54E-03
0.770376E-01
0.880783E-01
0.991436E-01
0.109468E 00
0.119768E 00
0.130660E.OQ
C.140886E 00
0-150074E 00
0.158373E 00
"""O. 165783'E 00
0.166985E 00
0.337610E-03
0.360613t-03
0.375432E-03
0.362259E-03.
0.326033E-03
0.360613E-03
0.365552E-03
0.316154E-03
0.29639AE-03
C.25687tjE-03 .
0.237115C-03
0.243702E-03
443
-------
S02 SORPTION RATE
8 31 71
RXT-7-3A
TEMPERATURE_= _ 20.^.000000. F
SPACE VELOCITY = 0.299944E 0'* /MR
INLET S02 MULE FRACTION (URY) * 0.002780
INLCT H20 MOLE FRACTION = __Q_._lOOpfi5 :
INLET OXYGF.N MOLE FRACTION = 0.035078
INLET co2 MOLE FRACTION = o.o
INLET NC MOLE FRACTION = 0.000149
INLET INERT GAS MOLE FRACTION * 0.862216
INLET CARBON WEIGHT = 27.289993 GMS
TOTAL GAS FLOW = 4.8 17.819__SC,FH.
(WET) -
0.002502
TIME
0. . _
30.
60.
90. _
120.
150.
1 HO - _
210.""
240.
..27Q._
300.
330.
-360.
390.
420.
__450.
480.
510.
.^520.
MOLE FRACTION S02
0.117000E-02
6.117000E-02
O.l'tlOOOE-02
0.144000E-02
0.153000E-02
0.168000E-02
h, l is?OOr>F-0?
0.180000E-02
0.177000E-02
0.186000E-02
0.194000E-02
0.188500E-02
.0.187000E.T02_
0.195000E-02
0.196500E-02
0.189000E-02.
0.196500E-02
0.208000E-02
0.2100.0QE-02,
H2S04 LOADING
GMS ACIO/GM C
RATE OF H2S04 SORPTICN
GMS 'ACID/GM C-KIN
0.0
0.159041E-01
0.306227E-01
0.440078E-01
0.568002E-01
0.684072E-01
0.795696E-01
0.901394E-01
0.999683E-01
0.109501E 00
0.118194E 00
0.126763E 00
, .0... 135.6.7.8 E. .00..
0.144272E 00
0.152397E 00
0.160818E 00
0.169240E 00
0.176722E 00
- _. 0.,. 1.7 3 9 9.4 E. 00
0.0
0.530136E-03
0.451109t-Q3
0.441231E-03
0.411596E-03
0.362205E-03
0.381961E-03
0.3226911: -03
0.332569E-03
0.302935E-03
C.276593E-03
0.294703E-03
672 7 3 300 E - 0 3
0.268361E-03
C.293056E-03
0.268361E-03
0.230494E-03
0.223908E-03
AVERAGE RATE OF S02 SORPTION
0.335513E-03
444
-------
$02 SORPTION RATE
8 31 71
RXT-7-4A
TEMPERATURE = 202.000000 F
SPACE VELOCITY = 0. 299954E~"~04 /HR "
INLL-T 502 MOLE FRACTION (URYJ = 0.002780
INLET H20 MOLE FRACTION = 0.100010
INLET OXYGEN MOLE FRACTION = 0.034786
INLET C02 MOLE FRACTION = 0.0
INLET NO MOLE FRACTION = 0.000149
INLET INERT GAS MOLE FRACTION = 0.862560
INLET CAKUUN WEIGHT = 24.750000 GMS
TOTAL GAS FLOW = A.369549 SCFH
(WET) =
0.002^02
TIME
MOLE FRACTION S02
H2S04 LOADING
GMS ACIO/GM C
RATE OF II2S04 SORPTION
GMS ACID/GM C-I'.IN
:".. 0 .
30.
60.
90.
1 120.
' iyO.
. 180.
210.
240.
270.
; 300.
330.
360.
390.
420.
450.
480.
510.
540.
570.
0.135000E-02
0.135000E-02
0.167000E-02
0.180000F:-02
0. 186000E-02
0* i*' >OvV^u"" O" C.
0.186000E-02
0.195000E-02
0.192000E-02
0.201000E-02
O.183000E-02
0.171000E-02
0.165000E-02
0.165000E-02
0.156000E-02
0.162000E-02
0.162000E-02
0.192000E-02
0.200000E-02
0.200000E-02
0.0
0.141270E-01
0.266733E-01
0.369969E-01
0.463819E-01
0.5502COC-C1
0.636702E-01
0.723143E-01
0.806620E-01
0.887133E-01
0.972093E-01
0.107187E 00
0.1180'34E 00
0.129217E 00
0.140825E 00
0.152581E 00
0.164041E 00
0.174018K 00
0.182119E 00
0.189825E 00
0.0
0.470900t:-03
0.365524E-03
0.322714E-03
0«3029t)6E-03
n > 7 J 7 I o c r> i
0.302956E-03
0.273319E-03
0.283198E-03
0.253561E-03
0.312835E-03
0.352351E-03
0.372110E-03
0.372HCE-03
0.401747E-03
0.38L989E-03
0.381989E-03
0.2H3198E-03
0.2b6n54e-03
0.2')6b54fc-03
AVERAGE RATE OF S02 SORPTION
0.327393E-03
445
-------
S02 SORPTIQN RATE
8 31 71
RXT-7-5A
TEMPERATURE =__?03.000QQp_JF ,_
SPACE VELOCITY = 0.299947E 04 /HR
INLET S02 MOLE FRACTION IUE_-JQ1...
0.9A8716E-01
0.103639E 00
0.1102>9E 00
0.116335E 00
0.121744L 00
.__0.126.700F 00
0.131228E 00
0.135452E 00
0.139602E 00
0.144047F 00
0.148493E 00
0_.J..52.7.9IE 00
0.157015E 00
0.206751t-03
RATL-
: H2S04
ACID/OK C-NIN
0..0
0.263462E-03
0.24b995E-03
0.276635E-03
0.246995E-03
0.2272.36^-03
0.256875E-03
0.227236E-03
0.204183E-03
0.246995E-03
0.246995E-03
0.263462.t-03
0.2272.36E-03
0.223942E-03
0.217356E-03
0.1fi7717E-03
0. 172097E-03
0. l^^07tE-0^_
0.143257L-03
0. 13U317L-03
0.13BJ17L-03
0. 15 HO 7 71: -03
0.138317C-03
0_. 14U197C-03
0. 133378F-03
446
-------
S02 SORPT10N RATE
8 31 71
RXT-7-6A
TEMPERATURE = 203.000000 F
SPACE VELOCITY *" 0. 299986E
INL1IT 5112 MOLE FRACTION (DRY)
INLET H?0 MOLE FRACTION =
INLET OXYGEN MOLE FRACTION =
IMLET C02 MOLE FRACTION =
INLET NO MOLE FRACTION = 0
INLET INERT GAS MOLE FRACTION
04 /HR
- 0.002760
0.099932
0.014928
0.0
.000150
0.862bl7
(WET) = 0.0024K-'.
INLET CARBON WEIGHT = 23.349991 CMS
TOTAL GAS FLOW = 4.122819
TIME _.MOLE FRACTION .502
0. 0. 163500E-02
30. 0.163500E-02
60. 0.171000E-02
90. 0.192000E-02
,-j. 120. 0.198000E-02
? 150. 0.204000E-02
ISO. 0. 1950CCE- 02
210. 0.198000E-02
240. 0.201000E-02
270. 0.213000E-02
i: 300. 0.207000E-02
: 330. 0.211000E-02
345. 0.210500E-02
360. 0.210000E-02
390. 0.216000E-02
420. 0.1.95000E-02
! 450. 0.205000C-02
* 480. 0.207000E-02
__ 510. .0..2.15QOOE-02
540. 0.19500QE-02
570. 0.195000E-02
600. 0.206000E-02
630. 0.204000E-02
660. 0.210000E--0.?
690. 0.207000E-02
710. 0.207000E-02
SCFH
H2S04 LOADING
CMS ACID/CM C
0.0
O.lll 160E-01 '
0.218615E-01
0.311990E-01
0.392026E-01
0.466133E-01
0.5*,1722E-01
0.620275E-01
0.695064E-01
0.764042E-01
0.829256E-01
0.695458E-01
0.927694E-01
0.96017BE-01
0.102243E 00
0.109209E 00
0.116718E 00
0.123635E 00
0.130057E 00
6.137073C 00
0.145076E 00
0. 152-5366 00
0.159552E 00
0.166370E 00
0.173039E 00.
0.177584E 00
RATE OF H2SO'( SOKPTION
CMS AC1U/GK C-J'IN
0.0
0.370535E-63
0.345832E-03
0.2/6666E-03
0.2'.>6904E-03
0.237142F-03
0.26t7S5i'-03
0.256904E-03
0.247023E-03
0.207'50CE-03
G.22/26H--03
0.214087E-03
0.215734E-03
0.217381E-03
0.197619E-03
0.266785E-03
0.233849E-03
0.227261E-03
_0.200912E-03
0.26f>785t--OJ
0.266785L-03
0.2305'55E-03
0.237142E-03
0.217381E-03
0.227261E-03
0.227261E-03
AVERAGE RATE OF 502 SORPT10N
0.24705/E-03
447
-------
APPENDIX A-16-2
SOo SORPTION RESULTS FROM DIFFERENTIAL RATE
APPARATUS FOR (NH4)2S EXTRACTED AND H2S
GENERATION CARBON SAMPLES
GRAVIMETRIC FLOW EXPERIMENTS
Run: 180-G SO?.:
Dry Weight: 95.10 mg NO:
Deflection: -6.18 mg. 02=
Carbon: Virgin, HgO:
C-70-7T
2000 ppm
150 ppm
3.5#
6.055
200°F
1500 cc/min.
75.11*
Correction: 0.1(907
Date: August 3, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
10
12
1>)
16
18
20
?5
30
35
1)0
1)5
50
60
70
80
90
100
330
120
330
11)0
150
360
170
180
190
200
230
2?P
230
2')0
250
260
270
280
290
300
Load
mg. HpSOlj/g. C
ll).72
37.35
39.35
20.93
22.08
23.fl)
2l) . 1(0
25.55
26.71
27.87
29-97
32.07
3l).17
36.38
38 . 1)9
Itl4.36
iio.aii
55.1)2
61.20
66.88
72.55
83.70
95-06
106.1)1
33.7.67
128 . 39
130.80
31)9.21
159-52
]6o.liO
379.18
380.06
198.32
207.36
215.77
223.76
231.1)1)
239.32
?1)6.27
253. 1(2
260.36
266.93
273-50
279.81
285.91
291.90
Mean Load
mg. HgSOlt/g. C
6
8
10
12
ll)
16
18
20
25
30
35
1)0
1)5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
ll)0
350
160
170
180
190
200
220
2l)0
260
280
300
Rate
HIR. H2S01t/g. C/min.
36.21)63
13.9327
11. 63 93
9.1(637
6.5720
3.2597
1.8822
1.5563
1.1672
1.0726
1.0726
1.1251
1.1356
1.1356
1.11)62
1.1567
.1 . 1 567
1.1567
1.1567
1.1567
1.1567
1.1567
. l.ii)62
1.11)62
1.1251
1.1 oia
1.0936
3.0726
1.0515
1.0305
1.0095
0_.9881)
0.9569
0.9253
0.8623
0.7886
0.7150
0.6309
0.51)68
448
-------
GRAV1MKTK1C FLOW
Run: 185-G
Dry Weight: 97.2U mg.
Deflection: -5-9^ me-
Carbon: RXT-6-3C
S02:
NO:
02:.
"20:
2000 ppm
150 ppm
6.07,
t:
Ft:
% IIpl.'Ol.:
Correction :
Date :
200°F
1500 en /win.
77-72
0.5076
August 20, 1971
Time
minute's
1
V
3
)i
c;
(>
7
8
9
10
12
Hi
16
18
20
25
OA
35
1(0
'(5
50
60
70
80
90
100
1.10
120
a 30
]1|0
350
160
170
100
190
POO
210
220
230
2'iO
250
260
2?0
?80
290
300
Load
mf,. }If>t:oj,/p:. C
5.55
8.6)-i
11 .00
1.3.27
J 5 . 3?
17. OY
18.9;'
20.57
22.21
23.76
26.1i3
29.21
31.78
3l*. 25
36.71
1)2.37
':7 . 72
52.55
57.28
61.81
66.23
7^.56
82.68
90.60
98.72
106. 6li
1 Hi. 66
12?. it 8
130.19
:i 37 70
I'i5.?.l
152. 'it
159-30
166. :i 9
173.08
179.86
186.65
193. '»li
199-9?
206 . 50
212.67
218.63
22'i.6o
230. !) 6
236.3''
21(1.88
Moiui Load
mg. Up;:/)],/,";. C
2
1|
6
8
'1 0
1?
Ill"
16
1H
20
25
30
35
)|0
'*5
50
rr
s s
60
65
70
75
80
85
90
95
100
110
120
130
ihO
150
360
170
l8o
190
200
220
2*40
Rate
rn.'-. Hp:/i)|/r:. 0/min.
5.01(12
it. 7306
3.77>42
3.":',37
2.1..V)P
2. fill)
2. 00 '".3
1.851-1
1.7277
] .621(8
1.1(500
1.3318
1.2230
1.1261
1.01490
0.9821
0.9255 ~"
0.8896
0.8536
0.8381
0.8227
0.812)4
0.8073
0 . 8021
0.7970
0.7970
0.7919
0.776*1
0.7610
0.7*156
0.7302
0.71)17
0.69)1?
0.6736
0.6582
0.61(27
0.5965
0.5502
449
-------
GRAVIMETRIC FLOW EXPERIMENTS
Run: 1B6-G
Dry Weipht: 101-70 mg.
Deflection: -6.35 mg.
Carbon: RXT-7-3C
NO:
H20:
2000 ppm
150 ppm
3.5%
6.0%
t:
Ft:
200°F
1500 cc/min.
75-56
Correction: O.li93li
Date: August 23, 1971
Time
minutes
]
2
3
lj
5
6
7
8
9
10
12
111
.16
.18
20
25
'.r>
35
1*0
1*5
50
60
70
80
90
HOG
110
120
330
.1.1)0
150
l6o
170
180
390
200
210
220
230
?1|0
2^0
260
270
280
290
300
Load
mg. H2SOl|/K. C
6.78
8.95
10.ll2
11.50
12.29
12.90
13.67
11*. 36
15 . Ok
15-73
16 .21
18.19
19.'i7
20.55
21.73
2l*.39
27.l'i
29.60
31.96
3l*. 32
36.68
1*0.90
1*5-23
1*9.16
52.90
56.M
60.28
61*. 01
67.1*5
71.1*8
75.22
79.35
83.1*8
87.1)1
91 .05
9k . 59
98.03
101.57
105.53
1 09.W)
113 .27
lif.ll
120 .9'i
121* . 78
128.1)2
131.86
Mean Load
ing. E2SOk/E- C
It
6
8
10
12
1>*
16
18
20
25
30
35
1*0
1(5
50
55
f$n
65
70
75
80
8=5
90
95
100
110
120
130
.
Bate
rag. HgSOli/fl. C/nrin.
5.5261
3.6185
2.26.16
1 . 37^6
0.8505
0.7030
0.6391
0.591*9
0.5605
0.5015
0.1(720
0.1)523
O.Ul25
0.1*277
0.1)228
0 . 1*179
O . 1(1 7Q
0.1)179
0.1*179
0.1*179
0.1)130
O.liOSl
0.1*031
0.3982
0.3933
0.3736
0 . 3589
0.3392
450
-------
GRAVIMETRIC FLOW CALCULATIONS
Run: 187-G
Dry Weight: 91.92 ing.
Deflection: -5-98 mg.
Carbon: RXT-7-5C
S02:
NO:
02:
HgO:
2000 ppm
150 pj)m
3.5#
6.0?
t: 200°F
Ft: 1500 cc/min.
% H2S01(: 75.83
Correction: 0.1)952
Date: August 2l), 1971
Time
minutes
1
2
3
1*
5
6
7
8
9
10
12
Ik
16
18
20
25
3n
35
1)0
1*5
50
60
70
80
90
100
110
120
130
ll)0
150
160
170
180
190
200
210
220
230
2)|0
250
260
270
280
290
300
Load
mp. UjjEOij/f-. C
7.29
1.0.K'
ia.97
13.27
in . 1*7
15. >*5
J6.l)3
17-30
18.06
18.71
19-9-1
21.00
22.19
23.39
21*. 1*8
27.09
90. ^0
31.98
33.9'+
36.01
37-86
1)1 .78
!)5.1»7
J)9 - ] 7
52.65
55- 92
59-10
62.66
65.93
68.97
7-1.91
75.17
78.1)1)
81.59
81*. 75
87-79
91.06
9't.-10
97.69
101.07
I0l).33
107.27
109.99
112.92
].15.5lt
117.93
Mean Load
mg. H2BOi,/g. C
1*
6
8
10
12
Hi
.1.6
18
20
25
30
35
1*0
1*5
50
55
60
65
70
75
80
85
90
95
100
110
120
,
Rate
mg. HpSOjj/g. C/trdn.
6.1)730
lt.7868
3.3616
2.T'08)|
1. Ii687
1.1151
0.8975
0.7398
0.636li
0.1*896"
0.1*569
0.')297
0.1*080
0.3916
0.3808
0.3753
0.3699
0.3590
0.3536
0 . 3l*8l
0 . 3372
0.3261)
0.3209
0.301)6
0.29^7
0.2665
0.2393
451
-------
GRAVIMETRIC FLOW EXPERIMENTS
Bun: 188-G S02:
Dry Weight: 100.66 mg. NO:
Deflection: -5-96 mg. 02:
Carton: RXT-6-5C HoO:
2000 ppra
150 ppm
3.555
6.0%
t: 200°F
Ff. 1500 cc/min.
% H2SOi,:' 76.97
Correction: 0.5027
Date: August 25, 1971
Time-
minutes
1
'i
t
3
!j
S
.. . £ . .
7
8
9
.10
12
111
16
18
20
25
on
35
1.0
U 5
50
60
70
80
90
100
:I.LO
120
130
I'lO
150
160
.170
180
J90
200
210
220
230
2lib "
2^0
260
270
2CO
290
300
Load
mg. Il2S01)/R. C
7.15
.10.53
13.31
15-50
37.6(1
19. 5Y
21 . 36
23.15
2>i.7)4
26 . 33
29 . 31
32.39
3'i.«7
37-55
liO.Oli
JJ5.90
n:n o£
J.IL. . ..^-
56.'i3
61.10
65.67
70 .Oil
78.1)8
86.83
9'i.87
102.52
109-97
117.23
12l).li8
131.53
138.1)9
I'i5.3l)
1 52 . 39
159.15
365.71
172 . 36
170. ft;1
iSli.ftB
390.611
136.70
202.56
20C.52
?l'i.39
220 . 1 S
225.91
23-1 .27
vtiM
Mean Load
m;-;. HoSOIj/g. C
If
6"
B ~
10
If?
Ill
. 16
18
20
25
30
35
1)0
'15
50
55
f,r\
65
70
75
80
85
90
95
100
110
120
130
lliO
150
160
170
180
190
200
220
?1|0
Rate
mg. HgSOli/g. C/iriiii .
6.3332
li.6U93
3.6956
3.0995
2.6376
2.37^3
2.1111
1.9'i22
.1.8180
1.5895
I.)i355
1.3:i63
1.2170
1.1276
1.01)81
0.993li
0 . 9li3ft
0.9090
O.G7l)2
0.81»9l*
0.8295
0.8lU6
0.79W '
0.7799
0.7699
0.7^51
0.7252
0.7053
0.690i|
0.6706
0.6557
0.6)i57
0.6259
0.61.10
0.591.1
0.5563
0.5166
452
-------
APPENDIX A-16-3
SULFUR GENERATION FROM 1 INCH DIAMETER FIXED BED
FOR (NH4)2S EXTRACTED AND H£S GENERATION CARBON SAMPLES
453
-------
RATF OF SULFUR GENERATION
BtNCH SCALE
RXT-6-IB
SPACE VELOCITY = 0.100125E 04 /HR
INFRT GAS FLOW RATE = 623.00 SCC/MIN
i^EIGHT OF CARBON, UNLOADED * 32.000 GHS
LOADED
INLET PERCENT H2S ~ 38.000
INLET MOLAR H2S CONCENTRATION -
INLET SULFURIC ACID LOADING =
0. 612903 MOLES H2S/MO_Lt
0. 1137600 CMS H2S04/GM CARBON,
l.68
_*P_-JLP.GMS
GAS
FINAL OUTLET PERCENT SULFUR LOADING ON CARBON =
4S FINAL OUTLET SULFUR LOADING ON CARBON = " 0.248~GMS S/GM CARBON
Ui INITIAL TEMPERATURE = 270.00 F
-!> MAXIMUM TEMPERATURE = 315.00 F
"FINAL TEMPERATURE = 310.00 'f
8 31 71
PERCENT S02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
PERCENT CO2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
MOLAR CONC H2S
0.0
0.214505E-01
0.219512E 00
0.199041E 00
0.319261E 00
0.562500E 00
0.612903E 00
0.612903E 00
H2S04 LOADING
GMS ACIO/GM C
0.187600E 00
0. 102135E 00
0. 322466E-01
-0.250390E-01
-0.752A60E-01
-0.996606E-01
-0.103237E 00
-0*!03237E 00
RATE ACID DECOMP.
GM ACIO/GM C-KIN.
0.0
-0.167B86E-01
-0.111666E-01
-0.1174776-01
-0.833515E-02
-0.143072E-02
0.0
0.0
TIME PERCENT H2S
0.0 0.0
5.0 0.2100006 Oi
10.0 0.180000E 02
15.0 0.166000E 02
20.0 0.242000E 02
_25.0 0.360000E 02
30.0 " 0.380000E 02
35.0 0.380000E 02
ACID LOADING - 0.1876bOE»01 AT0.111771E 02 MINUTES
RATE OF ACID DECOMPOSITION » -0.113034E-01 AT 0.111771E 02. MINUTES
AVERAGE RATE OF ACID DECOMPOSITION UP TO 90_PERC_ENT ACID UTILIZATION =
-O.I5696CE-01
-------
Ul
Ul
RATK OF SULFUK GENEKAHUN
BENCH SCALE
ri 31 71
RXT-6-2B
SPACE VELOCITY = 0.500870E 03 /HR
INERT GAS FLOW RATE » 291.00 SCC/NLN
_ME|GHT._QF. CARBON, UNL QA.D JE D_2 29.900 CMS
LUADEO
33.61 GMS
INLET PERCENT H2S ^ 32.000
LNLE_T_MOLAR_ H2S CONCENTRATION =
INLET SULFURIC *CID LOADING »
Q.47058B HOLES H2S/MOLE INERT GAS
0.139600 GMS H2SQ4/GM CARBON,
FJNAL Oj^f).EX.I^RGEN.T'SULFUR LQA01NG ON CARBON
FINAL OUHET, SULFUR LOADING ON CARBON -
INITIAL TiHPRATURE * 280.00 F
JLAXIMUM TEMPERATURE.; 300.00 F
FINAL TEHPERATURE = 298.00 F
15.420
0.184 GMS S/GM CARBON
TIME
PERCENT H2S
PERCENT S02 PERCENT C02
0.0 .
0.0
0.0
0.0
0*0
O.O
0.0
0.0
0*0
0.0
0.0
0.0
MOLAR CONC H2S
0.0
0.140251E
0.216545E
0:2903236
0.470588E
0.470588E
00
00
00
00
00
H2S04 LOADING RATE ACID DECOMP.
GMS ACID/GM C GM ACID/GM C-MIN.
0.139600E 00 .
0.827747E-01
, 0.4131326-01
0.104992E-01
-0.229061E-02
-0.229061E-02
0.0
-0.468745E-02
-0.360485E-02
-0.255795E-02
0.0
0.0
0.0
0.123000E 02
__0. 178000E__02
0.225000E 02
0.3200OOE 02
_._.0.320000E 02
ACID LOADING = 0.139600E-01 AT 0.288769E 02 MINUTES ^ ?
RATE OF ACID DECQMPQSLI JON j? -0_.2J>mM-0_2_ AJL.. a»_28,8769E _Ql_H.LNUTeS
AVERAGE RATE OF ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILISATION
-0.369408E-02
-------
Ul
RATE OF SULFUR GENERATION
BENCH SCALE
8 31 71
RXT-6-3B
SPACE VELOCITY = 0.^996025 03 /HR
INERT GAS FLOW RATE = = 293.00 SCC/MIN
WEIGHT OP CAHBONt UNLOADED = 30.120 CMS
LOADED
35.95 CMS
INLET PERCENT H2S = 32.500
INLET MOLAR H2S CONCENTRATION^
INLET SULFUR 1C AClD LOADING =
0.481481 MOLES H2S/MOUE INERT £&S
0.167100 GMS H2S04/GM CARBON*
FINAL Ot/TLET PERCENT SULFUR LOADING ON CARBON
FINAL OUTLET SULFUR LOADING ON CARBON -
INITIAL TEMPERATURE = 270.00 F
MAXIMUM 'TEMPERATURE^* HP_.00_F
'FINAL TEMPERATURE'- 298.od" r
17.910
GMS S/GM CARBON
TIME
PERCENT H2S
0.0
10.0
20.0
30.0
40.0
50.0
60.0
0.0
0.0
0.250000E 01
0.263000E 02
0.2750006 02
0.310000E 02
0.325000E 02
PERCENT S02 PERCENT C02 KOLAR
0.
0.
0.
0.
O.
0.
0
0
0
0
0
0
0.0
7100E-01 AT 0,,
0
0
0
0
0
0
0
oO
.0
.0
.0
.0
.0
.0
2 MINUJE.S_
0
0
0
0
0
0
0
CONC H2S
.0
.0
.256410E-01
.356852E
.379310E
.449275E
.481481E
00
00
00
00
H2S04 LOADING RATE ACID DECOMP.
GMS ACID/GM C GM AC1D/GM C-MIN.
0
0
0
-0
-0
-0
-C
. 167100E 00
.9881UE-01
.323407E-01
.882351E-02
.249071E-01
;- - -. - - ^ ,^_L-^ r ------ :
0.0
-0.682888E-02
-0.6465216-02
-0.
-0.
-0.
0.
176763E-02
144910E-02
456781E-03
0
ACID LOADING = 0
RATE OF ACID DECOMPOSITION = -0.468147E-02 AT 0.237971E 02 MINUTES
AVERAGE RATE OF ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION = -0.633341E-02
-------
RATE Of SULFUR GENERATION
BtNCH SCALE
RXT-6-4B
SPACE VELOCITY = 0.500339E 03 /HR
INERT GAS FLOW RATE = 287.00 SCC/MIN
Jrf.EIGHT.pF CARBON, UNLOADED_ 29.500 CMS
LOADED
36.69 QMS
INIET PERCENT H2S = 30.000
INLET MOLAR H2S CONCENTRATION =
INLET SUtFURIC AC 10 LOADING =
0.428571 MOLES_ H2S/MOLE_LNERJ_GAS_
0.185300 GMS H2S04/GM CARBON,
_F INAL_OUTLET PERCENT,SULFUR LOADING ON CARBON =
Ui FINAL OUTLET SULFUR LOADING ON CARBON
^J INITIAL TEMPERATURE » 305.00 f
_HAXIWUM TEMPERATURE * 311.00__f_ ___
FINAL tEMPERATURE » 297.00 F
1V.48Q
a 31 71
0.2<»2 CMS S/GH CARBON
TIME PERCENT H2S
-1 M ' '
0.0
15.0
30.0
45.0
60.0
0.0 , , .
0.8500QOE 01
0.223000E 02
0.262000E 02
0.300000E 02
PERCENT S02
0.0
0.0
0.0
0.0
0.0
PERCENT C02
0.0
OeO
0.0
0.0
0.0
MOLAR CONC H2S
0.0
0.928962E-01
0.287001E 00
0.355013E 00
0.428571E 00
H2S04 LOADING RATE ACID DECOMP.
GMS ACID/GM C CM ACID/GM C-MIN.
0.185300E 00 i
0. 103996E 00
0.532245E-01
0.303382E-01
0.225I27E-01
0.0
-0.476142E-02
-0.200812E-02
-0.104339E-02
0.0
-------
RATF DP SULFUR f.FNFRATION
BENCH SCALE
8 31 71
-P-
Ul
oo
RXT-6-5B
SPACE VELOCITY = 0.500410E 03 /HR
INERT GAS .FLOW RATE * 285.00 SCC/MIN
NEIGHf'OF'CARBON, UNLOADED = 29.280 QMS
LOADED,.?. 35._80 GM_S_
INLET PERCENT H2S = 34.200
INLET MOLAR H2S CONCENTRATION -
INLET SULFUR 1C ACID LCiADlNG~~=
OOE-Ol AT
S02 PERCENT CO2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.237^58E 02 MINUTES
MOLAR CONC H2S
0.0
0.204082E-01
0.695187E-01
0.43B849E 00
C.497006E 00
0.519757E 00
0.519757E 00
H2S04 LOADING
CMS ACID/GH C
0.186000E 00
0.775295E-01
-0.235415E-01
-0.800750E-01
-0.837527E-01
-0.8^5599E-Oi
-0.8^5599E-01
RATE ACID OECOMP.
GW ACID/GM C-MIN.
0.0
-0.708655E-02
-0.63896CE-02
-0. 114821E-02
-0.322871E-03
0.0
0.0
ACID LOADING = 0.1
RATE OF ACID DECOMPOSITION = -0.668019E-02 AT 0.237458E 02 MINUTES
AVERAGE RATE OF ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION = -0.693688E-02
-------
RATE OF SULFUR GENERATION
BENCH SCALE
8 3i 71
RXT-7-IB
SPACE VELOCITY = 0.494292E 03 /HR
INERT GAS FLOW RATE » 312.00 SCC/MiN
HEIGHT Of CARBONt UNLOADED ...... 32.410 GMS
LOADED
38.60 GMS
INLET PERCENT H2S * 26.800
1NLET MOLAR H2S CONCENTRATiON =
INLET SUIFURIC ACID~ LOADING "»
0.366120 MOLES H2J7 MOIE_ INERT GAS
0.167400 GMS H2S04/GM CARBON*
LlJS!AL.OUTLET PERCENT SULFUR LOADING ON CARBON
FINAL OUTLET SULFUR LOADING ON CARBON =
INITIAL TEMPERATURE = 273.00 F
MA_XIMUM TEMPERATURE _ 303.00 F
FINAL TEMPERATURE * 302.00 F ;
17,970
0.214 GMS S/GM CARBON
TIME PERCENT H2S
0.0 0.0
30.0 0.6500006 01
_60_. Q Q . 252 OQQ.E_fl2
90.0 0.256000E 02
105.0 0.268000E 02
ACID LOADING - 0
RATE OF ACID DECOMPOSITION
PERCENT S02
o.o . : :. .. .;,...
L 0.0 :-' .- :,:-s''-:. :
> 0.0
> 0.0
I 0.0
PERCENT C02 MOLAR CONC H2S
0.0 0*0
0.0 0.695187E-01
0.0 . 0.33689SE 00
0.0 0»?44086E 00
0.0 0.366120E 00
H2S04 LOADING
GMS ACID/GM C
0.167400E 00
0.278739E-01
-0.407232E-01
-0.5151-V3E-01
-0.538338E-01
RATE ACID OECOMP.
GM ACIO/GM C-MIN.
0.0
-0.416300E-02
-0.410U5E-03
-0.30926*E-03
0.0
L67400E-01 AT 0.3A8693E 02 MINUTES
5ITION = -0.355388E-02 AT 0.3^8693E 02 MINUTES
DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION = -O.A07793E-02
-------
-p-
ON
O
RATE OF SULFUR GENERATION
BENCH SCALE
B 31 71
RXT-7-2B
~SPACE VELOCITY - 0.615268E 03 /KR ~
INERT GAS FLOW RATE = 315.00 SCC/MIN
WEIGHT OF CARBON, UNLOADED = 26.330 CMS
LOADED
32.41 CMS
INLET PERCENT H2S = 26.300
INLET MOLAR H2S CONCENTRATION =
INLET SULFURIC ACID LOADING «
0.356852 MOLES H2S/MpLE__INERJ_GAS
6.168900 GMS H2S04/GM CARBON,
_FINAL OUTLET PERCENT SULFUR LOADING ON CAK80N
FINAL OUTLET SULFUR LOADING"ON CARBON =
INITIAL TEMPERATURE * 270.00 F
MAXIMUM TEMPERATURE = 315.00 F
FINAL TEMPERATURE * ~300JOO F
18.070
0.222 GMS S/GM CARBON
TIME
PERCENT H2S
0.0
0.0
0.0
0.400000E 01
0.230000E 02
0.245000E 02
0.260000E 02
0.255000E 02
0.260000E 02
PERCENT S02
0.0
0.0
0.320000E
0.300000E
0.0
0.0
0.0
0.0
0.0
0.263000E 02 0.0
ING = 0.168900E-01 AT 0
01
00
PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
o.o - ,
0.0 :
0.0
.295749E 02 MINUTES
MOLAR CONC H2S
0.0
0.0
0.0
0.417973E-01
0.298701E 00
0.324503E 00
0.351351E 00
0.342282E 00
0.351351E 00
0.356852E 00
H2S04 LOADING
GMS ACID/GM C
0.168900E 00
0.137777E 00
0.106655E 00
0.480550E-01
0.155062E-01
0.115598E-01
0.990935E-02
0.903412E-02
0.728368E-02
0.704382E-02
RATE ACID OECOMP.
GM ACID/GM C-MIN.
O.O
-0.622
-------
RATE OF SUI FIIK GENERATION
BENCH SCALE
8 31 71
RXT-7-5B
"SPACE VELOCITY = 0.500329E 03 /HR "~ ~'~
INERT GAS FLOW RATE = 237.00 SCC/MIN
__MilGH.L OF...CARBON»_ UNLOADED = 2*.320 CMS
;J LOADED
30.90 CMS
INLET PERCENT HZS = 28.000
INLET MOLAR H2S CONCENTRATION =_
INLET SULFURIC ACID LOADING -
0.388889 MOLES H2S/MOLE INERT GAS
0.18*000 CHS H2S04/GM CARBON*
_JF INAI._.OUTLET _PEJU:ENT SULJUR LOADING ON CARBON
FINAL OUTLET SULFUR LOADING ON CARBON
INITIAL TEMPERATURE = 270.00 F
MAXIMUM TEMPERATURE = 310.00 j
FINAL TEMPERATURE = 300.00 F
19*350
0.246 CMS S/GM CARBON
TIME
0.0
15.0
_30.0.
60.0
75.0
90.0
105.0
120.0
PERCENT H2S
0.0
0.1000QOE 01
0.800000E 00
0. 175000E 02
0.175000E 02
0.183000E 02
0.185000E 02
0.157000E 02
PERCENT S02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0,0
MOLAR CONC H2S
0.0
O.IOIOIOE-OI
0»806452E-02
0.212121E 00
0.212121E 00
0.223990E 00
0.226994E 00
0.1862AOE 00
0««28571£ 00
H2S04 LOADING
CMS ACID/GM C
: O.ie^OOOE 00
: 0.102195E 00
0.212486E-01
-0.975879E-01
-0.135261E 00
-0.171670E 00
-0.206<>9<»E 00
-0.2*5341E 00 :i
-0.256918E 00 ;
RATE ACID DECOMP.
GM ACID/GM C-M1N.
0.0
-0.538193E-02
-0.5*1086E-02
-0.251157E-02
-0.251157E-02
-0.234293E-02
-0.230025E-02
: -0.287930E-02
0.563822E-03
ACID LOADING = 0.184000E-01 AT 0.307191E 02 MINUTES
RATE_OF_ JVC. ID _DECOMPOS IT I ON. .= -0.53^137E-02 AT 0. 30 7191E 02 MINUTES
AVERAGE RATE OF ACID DECOMPOS'lTION UP TO 90 PERCENT ACIOUTILIZATION = -0.539510E-02
-------
APPENDIX A-16-4
(NH4)2S EXTRACTION EXPERIMENTAL RESULTS
RIM: RXT-T-1C
CARBON USED: RXT-T-1B
SOLVENT USED: 15?
Solution
Waiih Number
1
2
3
b
5
6
' T
6
9
10
i
2
3"
Time,
minutes
0
2
5
8
11
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
>
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5 -
10 -
15
0
5
10
0
5
10
0
5
10
Temperature ,
°F
100
102
105
105
105
120
111
110
103
105
102
105
108
110
107
107
105
102
101
102
100
115
ICO
100
103
120
105
105
105
105
107
100
100
110
100
105
100
115
108
105
105
95
100
110
110
105
110
305
105
105
Circulation Rate, ml./mln.
(NHIiJaS
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
91-
->^
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
H20
60
60
60
60
60
60
60
60
60
ml. (HE It) 28
Added
~50
-50
~50
50
-50
-50
^50
,-50
~50
-50
ml. (NHltJj: +
Sulfur Dralr.ed
19-5
36
37
36
3li.5
32
32
32.5
33
30
l46«
37*
39*
1. HjO Dr«in«4
After mtcr vmehlng, Bteamed for 2 hours at 1,000 cc/min.
462
-------
CA'UOIl I '.Ml: R»
Vftcli Kvjalwr
2
3
*
5
6
7
0
9
10
11
12
13
111
15
1
2
3"
T-7-2»
Time,
0
5
10
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
: J
10
15
0
5
10
15
0
5
10
3;
0
5
10
15
0
5
10
15
0
5
10
15
0
10
15
0
5
10
15
0
5
10
15
0
J
10
15
0
5
10
15
0
5
10
15
POLUTIOII arm: i^J (i.',:i,).,:! :;cjutlon
'!''.', iviiture ,
102
106
105
111
110
100
106
115
109
109
111 .
103
110
10k
109
115
105
105
J09
1X0
)00
110
103
117
100
109
105
120
100
102
123
100
110
98
112
110
105
111
110
110
69
106
110
100
110
102
111
111
112
103
110
110
90
100
112
90
110
110
310
327
105
110
110
120
111
111
111
i'"r ]~'^~ r '^j
35 '
35
35
Vi
35
.35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
60
60
60
60
60
60
60
60
60
60
60
60
p.!, (KIU,);;:
50
-50
-50
-50
-50
-50
-50
-50
~50
-50
-50
-50
-50
-50
~50
nl . (!i!l|,Nf! *
t'ul f'lf rr:»!no1
25
«2
25
llO
29.6
U6.2
53
51.5
1.2
1.8
1.8
lib
82.5
36.5'
!2.5«
66.3"
"After vater vn
it«nm«d for 2 hour* n,t 1,000 cc/mln.
463
-------
RXT-7-3C
CWKSI U1ED: BXT-7-3H SOLVENT USED! 151 (HIH^S Solution
V&Blt Itiunlitr
1
I
3
H
5
6
7
6
9
10
11
12
13
it
15
1
P
f"
Tlr,e,
rtltvit'e
0
5
10
15
0
5
10
15
0
5
ID
15
0
5
10
15
0
5
10
15
0
5
10
15
0
>
10
15
0
5
10
15
0
5
in
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
100
15
0
5
10
15
0
5
10
Ttfovcrriture,
T
105
102
105
105
112
100
106
100
110
100
IOC
10?
102
100
101
101
101
95
101
101
105
100
101
101
101
101
101
101
100
98
101
100
100
101
100
102
101
101
101
100
101
100
101
100
98
100
101
102
105
101
101
100
101
95
102
10?
110
100
lOli
102
103
101
101
101
100
101
101
100
100
105
101
Clrculitlon fljtlt.-, ri)./«.ln.
fuiiii)?;'
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
KiO
60
60
60
60
60
60
60
60
60
60
60
"''/JuM1*5
50
50
50
50
50
50
50
50
50
50
50
50
50
70"
50«
50-
Sulfur PrnlnM
16
1.5
51
U
1.8
U7
>*
50
VI
37
10
17
55
1,6
111."
U. IlpO A t>iuln-d
"After water vuolilng, ntnuw-il for 2 houra fit 1,000 cc/mln»
464
-------
RXT-T-liC
CARBON
BOIVHIT USEDi 15?
Solution
Vni.li llu«l«T
1
2
3
k
>
6
7
8
9
10
I
11
12
13
111
15
1
2
3"»
Time.
ml mi I* it
0
5
10
15
K .
10
»....
: o -
i 5 .0
10
W '...
0
5
19
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
Q
5
10
i;
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
J
10
15
Ttimjif ruture ,
Op
100
95
J101
101
105
101
102
102
110
102
103
103
100
103
103
103
110
10?
102
102
lOll
10?
105
105
95
100
100
100
106
100
101
IIS
91
95
1CI>
100
91
99
101
100
108
100
ICE
103
99
105
101
98
90
99
100
100
91
100
100
101
91
100
K'l
103
95
96
100
103
90
106
112
1H
190
126
J25
118
Circulation Fta
.. («!II,)?S
35
35
35
35
35
35
35
35
35
3?
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
te, nl./nln.
H?n
60
60
60
60
60
CO
60
Co
60
£0
ft) '
CO
Bl. (BnO?s
Aisled
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50"
50"
50"'
«ll. (KI!,,S .!: »
Sulfur I'rH, -1
52
n
i
1.9
1.7
1.9
51
51
1.8
U
53.5
S3
55
51
1.8
eo
Ii5«
59"
tg»
»1. ll?0 Added
1. II.-O llrtlnod
AftKr water wnahlnKi tpwned for t houra fti 1(000 cc/lnil).
465
-------
KSl! MT-1-5C
CARBON UGO>! RICT-7-5B
SOLVENT VSED: 15* (HH|,)zB Solution
V»h Kumber
1
2
3
14
b
6
7
8
9
10
31
ia
13
lit
15
1
2
Tln.e,
alni!t>>n
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
0
5
10
15
0
5"
10
i;
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
.15
0
5
10
15
0
5
10
15
0
10
15
0
5
10
15
0
5
10
15
Teir.s*ruture,
'f
100
es
90
103
100
100
109
10?
ICO
100
100
100
100
100
100
100
100
100
100
ICO
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
ICO
100
100
100
ICO
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Cliviil.alon lii
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
as
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
li-io "
65
«5
65
65
65
65
65
65
65
65
«5
6;
ml. (»i!i.):?s
AdiV>!
100
50
50
50
50
JO
50
50
50
50
50
50
50
50
50
100*
50"
50*
ml. (hMI.)?:'>
Rul fur IH-Rlnpd
1.9
1.6
111
50
59
50
19
60
1.8
1.2
50
1.3
*
50
56"
50"
1.6"
nl. ll.iO Added
*nl. H.,0 Druliioil
«»ft»r untcr vinli
utenmed for 2 Hour» »t 1,000 tc/«ln.
466
-------
KUHt RXT-7-6C
C/UIBOK USKD: SXT-T-6B
SOtVm USEDl 15*
Wash Humtwr
1
2
3
14
5
c
T
8
9
10
11
1?
13
ll>
15
1
i
3...
Time,
mlmiteg
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
JO
15
0
5
10
.ly
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
35
0
5
10
35
0
5
10
15
0
5
10
15
0
5
10
15
0
»
10
15
T> mpc r ttture ,
°F
100
120
100
100
100
100
100
100
95
100
100
100
100
100
100
105
105
105
105
105
110
105
100
100
95
100
100
100
105
100
100
100
95
100
100
110
95
100
100
100
95
100
100
100
105
100
100
100
105
100
100
100
95
100
100
100
105
100
100
ICO
100
10*,
105
105
105
105
111
110
110
110
..CJrcul.tlnn Rut
dim)-:!
35
35
55
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
e. »l.Mn.
M
60
Co
Co
60
to
£o
60
60
Co
CO
Co
60
nl. (NUl);S
91
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100"
50"
*'
ml. (HI! ) S «
1>5
19
1.6
16
5k
53
fc2
lift
57
H
50
51
k3
72
5P"
75"
ml. >l?0 AcMrd
"ml. lljO Umliied
"Aftrr vnur m>nlilnr,< lt««m"l fur ? houri
1,000 cc/Rln.
467
-------
APPENDIX A-16-5
PORE VOLUME DISTRIBUTION RUNS FOR (NH4)2S EXTRACTED
AND H2S GENERATION SAMPLES AFTER SIXTH CYCLE
SAMPLE: EXV-1
REL P
VOLUME
0. 1428
0. 1789
0.2149
0.3251
0.4313
0.5395
0.6477
0.7559
O.C641
0.9722
0.3628
0.3606
0.3733
0.3851
0.3950
0.4031
0.4103
0.41 6.8
0.4242
0.4350
S 667.4
C -22.544
R 0.9985
PORE RAUIU!
VOL
CUMV
1000.
500.
400.
300.
200.
150.
10U.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
13.
16.
14.
12.
10.
0.0022
0.0009
0.0014
0.0024
0.0022-
0.0040
0.0012
0.0015
0.0019
0.0025
0.0034
0.0023
0.002H
0.0035
0.0047
O.OOfO
0.0115
0.0071
0.0096
0.0123
0.0149 '
0.0204
0.0022
0.0031
0.0045
0.0070
0.0092
0.0131
0.0144
0.0159
0.0178
0.0203
0.0237
0.0260
0.0238
0.0323
0.0369
0.0439
0.0554
0.0625
0.0721
0.0044
0.0994
0.1198
468
-------
SAMPLE: RXT-6-6C
REL P
VOLUME
0.1487
0.1863
6.2238
0.3365
0.4492
0.5619
0.6745
0.7872
0.8924
0.9900
S
C
R 0.
0.4417
0.4461
6.4532
0.4688
0.4794
6.4838
0.4922
0.4995-
0.5075
0.5156
794.2
-20.632
9986
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0006 ..
0.0004
0.0008
0.0017
0.0018
0.0037
0.00i2_
0.0015
0.0020
0.0026
0.0037
0.0024
0.0030
0.0039
0.0059
0.0081
0.0058
0.0043
0.0100
0.0153
0.0215
0.0301
0.0006
0.0010
0.0018
0.0034
0.0053
,- '0.0090
. ._.. 0.01 0.2...
:o.oii7
0..0137
0.0163
0.0199
0.0223
0.0253
0.0292
0.0350
0.0431
0.0489
0.0532
0.0632
0.0785
0.1000
0.1301
469
-------
SAMPLE: RXT-7-6C
REL P
VOLUME
0.1487
0.1863
0.2238
0.3365
0.4492
0.5619
0.6745
__0.7872
0.8999
0.9900
0.3417
0.3490
0.3530
0.3646
0.3742
0.3823
0.3895
0.3959
0.4031
0.4099
S 617.8
C -20.604 _
R 0.9983
PORE RADIUS
VOL
CUMV
1000.
500.
400.
_ .300.
200.
150.
IOQ*_
90.
80.
70.
60.
50.
45.
40.
35.
_ . 30.......
25.
20.
18.
16.
14.
12.
_ 500.
400.
300.
._200.
150.
100.
9.0,
80.
70.
60.
50.
45.
.40.,
35.
30.
25.
20.
18.
16,
14.
12.
10.
0.0008
0.0004
0.0007
0.0015
0.0016
0.0031
,.Q,OQIO _
0.0013
0.0016
0.0022
0.0031
0.0021
. 0,0026..
0.0034
0.0047
0.0070
0.0112
0.0071
0.0093 _
0.0119
0.0147
0.0185
0.0008
0.0012
0.0020
0.0034
0.0050
0.0081
0,009}
0.0104
Oo0120
0.0142
0.0173
0.0194
__.0.,0220_
0.0254
0.0301
.___0..0371
0.0483
0.0554
, 0^0647:
0.0766
0.0914
0.1099
470
-------
APPENDIX A-17
POST-TREATMENT RESULTS OF AMMONIUM SULFIDE SOLVENT
EXTRACTED CARBON
1. Experimental Conditions for Isothermal and 472
Thermal Post-Treatments of (NH4)£S Extracted
Carbon
2. Experimental Results for Determination of the 475
S02 Activity of Post-Treated (NH4)2S Extracted
Carbon Samples Using Differential Rate
Apparatus
3. S02 Sorption Rates for Determination of the 486
S02 Activity of Post-Treated (NH4)2S Extracted
Carbon Samples Using Differential Rate
Apparatus
471
-------
APPENDIX A-17-1
EXPERIMENTAL CONDITIONS FOR ISOTHERMAL AND
THERMAL POST-TREATMENTS OF (NH4>28 EXTRACTED CARBON
RUN NO.:
TYPE CARBON:
DESCRIPTION OF RUN:
EXPERIMENTAL CONDITIONS:
RXT-T-6C-1
RXT-7-6C
Run at 1000°F for 2 hrs. with 30% H2
Weight of Carbon: 0.5 gms
Bed Temperature: 1000°F
Inlet H2 Concentration: 30%
Gas Flows: N2 - 19A cc/min.; H2 - 8.3 cc/min.
RUN NO.: RXT-7-6C-U
TYPE CARBON: RXT-T-6C
DESCRIPTION OF RUN: Run at 800°F for U hrs. with H2; 2 hrs . preheat time
EXPERIMENTAL CONDITIONS: Weight of Carbon: 0.5 gms
Bed Temperature: 800°F
Inlet -H2 Concentration: 305?
Gas Flows: N2 - 19-U cc/min.; H2 - 8.3 cc/min.
RUN NO.:
TYPE CARBON:
DESCRIPTION OF RUN:
EXPERIMENTAL CONDITIONS:
RXT-T-6C-5
RXT-7-6C
Run at 1200°F for k hrs. with H2; 2 hrs. preheat time
Weight of Carbon: 0.5 gms
Bed Temperature: 1200°F
Inlet H2 Concentration: 30%
Gas Flows: N2 - 19.!+ cc/min.; H2 - 8.3 cc/min.
472
-------
RUN NO.: RXT-7-6C-6
TYPE CARBON: RXT-7-6C
DESCRIPTION OF RUN: Run at 1000°F for U hrs. with H2
EXPERIMENTAL CONDITIONS: Weight of Carbon: 0.5 gms
Bed Temperature : 1000°F
Inlet H2 Concentration: 30$
Gas Flows: N2 - 19.^ cc/min.;
H2 - 8.3 cc/min.
RUN NO.:
TYPE CARBON:
DESCRIPTION OF RUN:
EXPERIMENTAL CONDITIONS:
RXT-7-6C-7
RXT-7-6C
Run at 1000°F for U hrs. with N
Weight of Carbon: 0=5 gms
Bed Temperature: 1000°F
Inlet H2 Concentration: 0
Gas Flows: N2 - 27-7 cc/min.;
2 hrs. preheat period
H - 0
RUN NO.:
TYPE CARBON:
DESCRIPTION OF RUN:
EXPERIMENTAL CONDITIONS:
RXT-7-6C-8
RXT-7-6C
Run at 1000°F for
Weight of Carbon:
hrs. with CO; 2 hrs. preheat period
0.5 gms
Bed Temperature: 1000°F
Inlet CO Concentration:
Gas Flows: N2 - 19-^ cc/min.;
CO - 8.3 cc/min.
473
-------
RUN NO.:
TYPE CARBON:
WEIGHT OF CARBON:
DESCRIPTION OF RUN:
RXT-7-6C-9
RXT-T-6C
0.5 gms
(1) Washed for 15 minutes with 50 ml. of a 2% NH^OH solution
at 77°F
(2) Three distilled H20 washings of 50 ml for 15 minutes
each at 77°F
(3) Heat the sample in a 1,000 scc/min. purge of N2 for
1 hour at UOO°F
RUN NO.:
TYPE CARBON:
WEIGHT OF CARBON:
DESCRIPTION OF RUN:
Virgin Washing with
Virgin, C-70-77
0.5 gms
Same as RXT-7-6C-9
474
-------
APPENDIX A-17-2
EXPERIMENTAL RESULTS FOR DETERMINATION OF THE S02
ACTIVITY OF POST-TREATED (NH4>2S EXTRACTED CARBON
SAMPLES USING DIFFERENTIAL RATE APPARATUS
475
-------
CAICULATIIINS fUK &KAVIHIIHIl flllM l«l'lH|MlNli
MUM NO.
UMl
UKV Hl.>
COKRtUION-
Tint
(MINI
1.00
^ 2.00
3.00
4.00
5.00
6.00
7.00
6.00
9.00
10.00
11.00
12.00
13.00
14.00
15.00
16.00
1 7. 00
18.00
19.00
20.0(1
21.00
22.00
. . 23.00
24.00
25.00
... . 26.00..
27.00
28.00
29.00
30.00
33.00
36.00
, 39.00
42.00
. 45.00
48.00
51.00
. . .5-4.. 00
57.00
60.00
63.00
66.00
69.00
72.00
' 75.00
78.00
. - ...Bl.OO.
84.00
87.00
.'.^. ..90.00
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144.00
150.00
156.00
162.00
168.00
174.00
180.00
IH6.00
142.00
198.00
204.00
210.00
216.00
222.00
22K.OO
2J4.00
240. 00
246. DO
252 . f'U
25H.OO
264.00
270.00
276.00
tH/.PO
2rlil.n(i
244 .5200
0.5200
0.5200
0 5200
0.5200
0.5200
0.5200
0.5200
0.5200
. ......0..5200.
0.5200
0.5200
0.5200
0.5200
0.5200
g.5200
0.5200
0.5200
_. 0,5.200.
0.5200
0.5200
0.5290
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5206
0.5200
0.5200
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650'
0.5650
0.5650.
0.5&50
0.5650
0.5650
0.5650
0.5650
.0.565J
0.5650
0.5650
0.5650
0.6050
0.6050
0.6050
O.fcO'-O
0.605D
P.W50
0.6'J^l)
0.6.150
0.6.1MI
O.M'M)
C.fcC'M
O.CPIO
11.KI50
0.<*>>SO
. _ D.6050
O.hOSO
P.C..1SO
0. 6^50
O.M'SO
2000. PPM HUP
150. PPK Fl 'I "
J.5 < M2iU4 *
6.0 I
CHART
INCHES
7.40
8.0A
8.16
B.27
8.36
8.49
8.60
8.70
8.80
B.91
9.0.2...
9.14
9.22
. . . . ... ..9-31 .
9.42
0.52
0.62
0.71
0.81
0.91
1.02
1.14
.25
.36
.47
*58
.69
.79
J.90
2.00
2.32
2.66
2.98
3. JO
j ,63
).9~6 '
4.28
4.60
4.91
5.23
5. 56
5.89
6.21
6.52
6.86
7.19
7.51
7.83
8.16
B.47
8.79
9.10
0.34
0.66
0.97
1.27
1.57
1.87
2,11
2.47
3.05
3.62
4.19
4.77
5.32..
5.88
6.41
. _ .._ 6.95 .
/.49
8.00
8.59
0.45
1.41
1.85
2.24
2.72
3.15
4.56
1.97
4.J8
4.77
5.16
5.54
5.42
6.24
6.66
7.0U
1. 11
1. 11}
8.04
2OU. DIG. r.
15CO. CC/MIN
75.14 S
PICKUP
IMG H2SO4I
1.61998
. 1.75998.
1.87997
1.9N947
2.09996
2.20998
2.3149U
2.4199B
2. 51997
2.62997
Z. 73997
2.B5999
2.93997
3.0299U
" 3.I399S
3.2.3997
i. 13998
3.42998
3.52998
J. 62997
3.7S9V7
3.80999
3.96999
4.07997
4.U997
r 4., 2999.1.
4.40197
4 ,,5099 8
. 4.61998
4.71999
5.03998
5,37997
5.69998
6.01997
6B3'*990
6. 67990
6.99998
7.31998
7.62997
7.94^40
8.27998
0. 60999
8.92998
9.23997
9.57997
9.90997
10.22998
10.54997
10.87997
11.1H997
11.50998
11.81998
12.05998
12.37997
12.68997
12.98997
13.28998
13.5B998
. J 3. 88998
14.18997
14.76997
. _ 15.3)998
15.90997
16.48997
17.03998
17.59998
18.12997
_. . 16.66998
14.20908
19.71999
20.21494
20.66448
21.12497
2 1.56-148
22.00448
22.41497
22.8649ft
23.27998
21.6H44T
."4.09498
24.40941
24.67497
25.2549S
2"1 . 6 J44H
20.00146
2I>. 71944
27.0H'I'IU
21.419'iH
2 7. 7*i *'IU
476
-------
tALUIlAIIIUll II.K u
Ull. rili
RUN NM. »
DA 11 «
DRY WT..
COKREC HUN-
TINE
l.CO
z.oo
3.00
4.00
5.(/0
6.00
7.00
8.00
9.00
10.00
11.00
12.00
13.00
.14.00 ..
15.00
16.00
17.00
18.00
19.00
.20.00
21.00
22.00
J3.00
24.00
2'*. 00
26.00.-
27.00
28.00
... 27.00 .
30.00
33.00
_.. J6.DO
39.00
42.00
45.00
48.00
91.00
.. -SA.OO .
57.00
60.00
63.00
66.00
69.00
72.00
75.00
78.00
SI. 00
84.00
87.00
90.00
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144.00
150.00
156.00
162.00
168.00
174.00
1HO.OO
lUh 00
192.00
1 9ll. 00
204.00
210.00
216.00
222.00
22(1.00
234. PO
240.00
246.00
252.00
2SH.OO
2*4.00
270.00
2 H«. UO
2H2.00
2HH.OO
2V4.1'0
300.00
189 ',11,- .
8 31 U 1411 *
1H.KI, MG , 02 *
-6.22 HG 1120 »
HASS DIM
0.4'JOO
. _ O.'t'JOO
0.4900
'J.1,'100
O.VIOO
0. VJOO
0.5.300
. 0.5300
0.5100
0.5300
_ 0.5100
0. 5JOO
0.5300
. .. . ...0..5300
D.4300
0.5300
0.5300
0.5300
0.5300
0,5300
0.5300
0.5300
0..5300..
0.5300
0.5300
_. 0. 5300..
0.5300
0.5300
. 3.5300
0.5300
0.5300
, a, 5300.
0.5300
0.5300
0.5300.
0.5300
0.5300
0.5300
0.5300
O.'iJOO
0.5300
0.5300
0.5300
0.5300
0.5300
0.5300
0-5300
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5900
. 0.5400
0.5900
0. 5900
0.5900
0.5900
0.5900
0.5900
J.4900
0.5900
d . 5900
0 . 5900
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0.4900 .
0. V'OO
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c.vioo
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0.6400
0.6400
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0,6400
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2'IOU. I'M* l| HP 200.
150. IM'H ||!| 1500.
3.4 T II21IJ4 = 75.55
6.0 X
i it AH r
7.60
.._ 7.9} :
8.18
8.311
H. 56
B.72
0.86
. 1.03
1.21
1.37
1.53
1.69
1.85
?,00
2.17
2.32
2.47
2.6f
2.77
_ -. -2..9.Q ..
J.02
3.16
... _. 3,20 _ .
3.40
3.50
... ._ .3,60 i
3.70
3.80
_ .. 3i90.
3.99
4.34
... ._ 4.65 .
5.00
5.31
5,61
5.92
6.21
6n51
6.81
7.10
7.39
7.68
7.97
8.25
8.52
8.81
9..09
0.30
0.59
0.87
1.16
1.43
1.71
1.99
2.26
2.54
2.81
3.09
... 3.35
3.61
1.09
.1.63
2.17
2.69
3.20
3.71
4.22
4.73
5.21
5.64
6.17
6.66
7.16
.f.64 . ..
11.13
H.61
4.08
9.44
10.00
0.40
O.K3
1.26
l.6t>
2.09
2.49
2.lt9
3.27
3.65
4.U2
4.^0
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Ct/hIN
I
PICKUP
(KG M2504)
0.51999
0.829 ft
.09999
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2.1299V
2.45000
2.60-199
2,76999
2.92000
3.09000
3.23999
3.3H998 _
3.52998
1.60999
3,81999
3,93')99
4.01999
. . .. ,«.«. 20000
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4.42000
A.51S.9S
4. (2000
4i71999
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4,90999
5.25999
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5.92000
6.23000
6,52993
6.84000
7.12999
7,42997
7.7300C
n. 01999
8,31000
8,59999
8.8H998
5,17000
9,43999
9.73000
10., Q099?
10.21999
10.50999
'10.78999
11.07999
11.34999
11.62999
11.90994
12.17999
12.45999
12.73000
13,00999
13.26999
13.52998
14.00999
14.54999
15.09000
15.60999
16.12000
16,62999
17.13998
17.64999
18.12-J94
18.60999
1 9. 09000
19.57999
20.0f999
20,56000
21.04999
21.52998
21. 90998
22.4S999
22.92000
23.31999
23.74-)')B
24.17999
24.59999
24.009*»9
2">.409'»9
5.111000
6. l(l'»99
6.46'»99
|..'M-I'I9
7. .1 1 V9
477
-------
rc..< I,H/WH'[ i
RUH Nil. 191
(Mil 1 2 It .
ORY WT.- 100.56 PC
CURRCCTIUN* -6.43 Ht
HUE
(MINI... ...
1.00
2.00
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
11-00 . .
12.00
11.00
.. .. 14.00 ._ . .
15.00
16.00
17.00
18.00
19.00
20.00
21.00
22.00
. .23.00
24.00
25.00
26. OQ
27.00
26.00
29.00
30.00
33.00
36.00
39.00
42.00
45.00
46.00
51.00
. . 54.0O
57.00
60.00
63.no
66.00
69.00
. .72.00 _
75.00
78.00
... 61.00
84.00
87.00
90. on
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144.00
150.00
156.00
162.00
168.00
174.00
180.00
1H6.00
19?. 00
I9H.KO
204.00
210.00
216.00
222.00
228.00
234.00
240.00
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252.00
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264.00
270.00
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2C2.00
2H".00
294.UO
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MASS DIAL
0.5000
0.5000
0.5000
0»5000
0.5000
0.5009
0.5000
... 0.5000
0.5000
0.5000
0.5000
0.5450
0.5450
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0.5450
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0.5450
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0.5850
0.5850
0.5650
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8.05
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U.58
8.73
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9.01
9.15
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2.97
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3.44
3.66
3.87
4.09
4.30
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4.72
4,93
5.1*
5.34
5.55
.... ... . 5.75
5.95
6.15
6.35
6.5*
6.73
6.91
7.10
7.29
7.46
7.66
7.8*
8.02
8.20
8.56
0.93
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0.6/'>e
0. t>2'>0
il.(,.".0
O.h2'»0
ll.l/Sl)
O.f. 2'tO
II. (.">('
U.I.,' '.0
I EMP '
Mil -
M2SU4
CHART
IMCMFS
7.49
7.69
7.88
8.04
8.20
«. 35
8.50
8.63
8.76
8.b9
9.01
9.12
9.23
....0.2'. .
0.35
0.46
0.56 .
0.66
0.76
.0.87.
0.97
1.06
-1.14
1.24
1.34
1.43
1.51
1.59
i.«.69._.
1.78
2.04
4,29,
2.54
2.79
3,04
3.29
i.53
JU 78
4.0l"
4.25
4.49
4.72
4.96
5.19
5.43
5.66
5.9.0
6.13
6.36
6 so
a. 82
7. Ob
7.30
7.54
7.77
8.00
8.23
8.46
S.69
3.91
4.36
C.tll
1.27
1.7)
2.18
2.62
3.06
. I.4B
0.40
l.il
1. /O
2. I'l
.' . t.O
I.UI
1.44
I.H6
. / '1
4. 10
*.! 1
I
'..'11
^. 1U
t. . l> -1
i.PI
1.44
7 »ll 2
t . 1 li
C.1)*
I'.ni
'i . .' 3
200. ore. F.
1M.O. CC/MIN
76.92 I
PICKUP
(Mb H2SII4I
0.91997
1.11996
1.30447
1.46947
1.62997
1. 77947
1.4249S
2.05997
2.18947
2.3194*
2.43497
2.54497
2.65997
2.66497.
2. 77997
2.88997
2, 989') 1
3.08997
3. 18997
3.29997
3.34496
3.48997
3.56948
3.66-197
3.76997
, .3. 5)5947. . .
3.43997
4.01997
. ...4 ,11 9-9 6
4.20998
4.46997
4.71997
4.9690.7
5.21997
5.46997
5.71997
5.95998
...... 6, 2099B... __
6.43997
6.67998
6.91997
7.14996
7.38997
7,61996
7.85997
8.06997
8.32997
t. 55997
8.78996
9.01997
4.24997
9.50996
9.72997
4.46447
10.19997
10.42998
. ' 10.65997
10.88997
11.11996
11.33947
11.78996
12.23997
12.69997
13. 15997
U.60'197
14.04'I9;
ll.4H')9(
14.9099/
1 '< . 3/'l94
15. 759-IB
lo. IB'l I'l
16.619 IB
1 7.079'IB
If. 4 »>(»
17. Hf.'llIH
If .2H44H
If. /1'1'W
14. 1,"|.| 1
I'l .5 I'HH
l'l.9 ).|'I4
2f. ll'l'ld
20. /24'lrt
21. 1 1'1'IH
21. 4'lrl'IB
21.H(,'M,1
22. '4'l9il
/,'
-------
IALCUIAI IDNS ru« GKAVIMHRIC HUW
HUN NO. 196 502 2000. PPM
DATE 9 14 71 (W » lr>q. PPH
DRY HI.- 100.42 HC O2 3.5 »l
COKRECtlON' -6.22 MO H20 6.0 I
TIME
. .IMINI
i.oo
..2.00..
3.00
4.00
...5,00
6.00
7.00
8.00 _
9.00
10.00
. . 11.00 . . .
12.00
13.00
._.14.00
15.00
16.00
. . _..17.00
18.00
19.00
20.00
21.00
22.00
.. _ 23.00
24.00
25.00
_ ..26.00
27.00
28.00
29.00
30.00
33.'00
36.00
39.00
42.00
4 5.. 00
48.00
51.00
54.00
57.00
00.00
63. .00 .. _
66.00
69.00
17.00
75.00
78.00
81.00
84.00
87.00
90. nn
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
120.00
126.00
132.00 . .
1 Jfl.OO
144.00
150.00
156.00
162.00
168.00
174.00
IbO.OO
186.00
192.00
198.00
204.00
210.00
216.00
222.00
228.00
234.00
240.00
246.00
2*2.00
264.00
270.00
? IA nn
2B2.00
288.00
294.00
300.00
MASS DIAL
0.5000
O.SOOO
0.5000
0.5000
,0.5000..._
0.5000
0.5000
.. . 0.5000
0.5000
0.5000
. . 0.5000
0.5000
0.5000
..... ... . _0,5000 . .
0.5000
0.5000
0.5.00D
0.5000
0.5000
0.5000
0.5000
0.5000
. 0.5000
0.5000
0.5000
p. 5000
0.5000
0.5000
o.r,ooo
0.5000
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5-400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400 .
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
9,5400..
0.5400
0.5400
0,5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.540Q
0.5400
0.5400
0.6400
0.5400
0.5400
0.5400 _ ...
0.5400
0.5400
_ 0.5400 _ ...
0.5400
0.5400
0.5400
0.5400
0.5400
0.540D
0.5400
0.5400
0.5.400 . _
0.5400
0.5400
0*5400
0.5400
n»f > 200. ore,. F.
f 1 [| 1500. CQ/MIN
t«S04 75.78 I
CHART 1
HIGHER (M!
7
7
7
7
7
7
7
f
7
7
a
8
8
8
8
8
8
8
8
8
8
8
8
8
8
a
8
8
8
8
0
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
.44 (
.54 (
.60 !
.65
.71
.77
.82
.88
.93
.98
.04
.10
.16
,2_1.
.26
.31
.36
.40
.44
19
.54
.59
.63
MCKUP
;_ii2S04)
). 79999
1.89999
). 95999
.00999
.06999
.12999
.17999
.23999
.28999
.34000
.39999
.45999
.51999
.56999
.62000
.67000
.71999 ___
.75999
.79999
.84999
.89999
.95000
.98999
.68 2.03999
.72 2.07999
.76 2.120DO
.so ;
.85 i
'.}} ";
.93 i
,0.3 <
.14 i
.26 i
.37 i
.48 ;
.59 i
.6? 3
.79 :
.69 :
'!'09 3
.19 :
.29 5
'.15999
'.20999
'.25000 .
'.28999
'.28998
'.38998
.49998
.61998
.72998
'.83998
'.94993
1.04997
1.14998"
.3499B
1.44998
1.54997
.64998
.39 3.74998
.49 3.84998
.59 3.94998
2.69 4.04997
2.78 4.13998
2
3
3
3
3
3
3
3
3
3
3
4
4
4
4
4
4
5
5
5
5
5
6
. 6
6
J»
6
6
7
7
7
7
.7
7
8
,.. 8
a
8
. 8
.97 4.32997
.06 4.41998
.15 4.50998
.24 4.59998
.32 4.67998
.40 4.75998
.49 4.84998
.57 4.92998
.66 5.01997
.74 " 5.09990
.90 5.25998
,08 . . 5.43997
.26 5.61998
.44 5.79997
.61 5.96997
.80 6.15997
.98 6.33998
,16 , 6;51997
.34 6.69998
.51 6.86998
.70 7.05998
.87 7.22998
.05 7.40997
.72 7.57997
.40 7.75998
.58 7.93997
.75 8.10999
.93 ~ 8.28998
.10 8.45998
.27 ....... ..8.62997
.43 8.789V8
.60 8.95998
-77 9.12997
.94 9.29997
.10 9.45998
.27 9.62997
.44 9.79997
.60 9.95998
.77 10.12997
B.91 10.28998
483
-------
CALCULATIONS FUR GKAVIMUHIC HI,.! CXI'CHlMbNTS
RUN NO.
DMt
DRV Hi.-
COHRfCT ION"
TIME
I«!NI
1.00
2.00
3.00
4.00
5.00
6.00
7.00
. 8.00
9.00
10.00
1KOO
12.00
13.00
14.00 .
15.00
16.00
17.00
18.00
19.00
20.00
21.00
22.00
23.00
24.00
25.00
__26.00_. .
27.00
28.00
29.00
30.00
33.00
36.00
39.00
42.00
45.00
48.00
51.00
S4.00
57.00
60.00
63. 00
66.00
69.00
J2.0.0 _
, 75.00
78.00
fll.nn
84.00
87,00
on. on
93.00
96.00
99.00
102.00
105.00
100.00
111.00
114.00
117.00
120.00
126.00
132.00 .
\iU.UO
144.00
_. 150.00
I5(..<>0
162.00
168.00
174.00
180.00
106.00
192.00
198.00
204.00
210.00
216.00
222.00
228.00
234.00
240.00
246.00
757.00
2b.a.co..
264.00
270.00
216.00 .
282.00
200-00
294.00
300.00
197 S02 2000. PPM
9 15 71 _ HI) » j 50. PP«
Vfl.30 MC 02 "" 3.5 X
-6.09 MC H20 6.0 »
MASS DIAL
0.4900
0.4900
0.4900
0.4900
0. 4VOO
0.4900
0.4900
.. 0,4900 .
0.4<)00
0.4900
0.4900
0.4900
0.4900
0.4900
0.4'!00
> 0.4900
O.',900
0.4900
0.4900
0.4900
0.4900
0.4900
0-4-(00
0.4900
0.4900
0.. 4.90.0
0.4900
0.4900
0.4900
0.4900
0.5350
0.5J50
0.5300
0.5350
0.5350
0.5?50
0.5350
0.5*50
0.5350
0.5353
0.5300
0.5350
0.5350
0.5350 , ,
0.5350
0.5350
0.5350
0.5350
0.5)50
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
. . . 0.5359 _
0.5350
0.5350
0.5}',0 _. .
0.5350
0.5350
0.5350
0.5350
0.5350
_0.535Q
0.5350
0.5350
0,5350
0.5350
0.5350
0.5)50
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5J50
O.S1SO
O.SJSO
IfHf 200
FID « ...151.0.
112 SO* " /4.73
CHART
INCHC-S
7.52
7.63
7.70
7.77
7.83
7.89
7.96
_...8,P2
8.09
8.15
8.21
8.28
8.34
8.40
8.45
8.50
8.54
8.59
8.64
8,69
8.74
8.78
8.8? .
8.116
8.90
..J1..94
B.9B
9.02
9.07
9.11
0.08
0.19
0.30
0.41
0.52
0.62
0.73
0.83
0.93
!.04
1.1 'i
1.25
1.36
1.47
1.57
1.67
1.77
'..86
1.96
2.06
2.15
2.25
2.35
2.45
2.55
2.65
2.74
2.84
7.93
3.01
3.20
_.- ».»«.. _ .._
3.57
3.75
,.3.93.
4. 10
4.30
4_,48
4.65
4.02
5.00
5.18
5.35
5.52
5.70
5.88
6.06
6.24
6.42
6.60
6. BO
6.98
'**,
7.35
7. S3
7.70
7.89
8.07
6.23
8.39
. OEG. F.
CC/MIN
I
PICKUP
(Hb H2SU4I
1.12997
J.2399.7_ _
1.30998
1.37997
1.43997
1.49998
1.56998
1.62997
1.6999!)'
1.75998
1.B1998
1.88998
1.94998
2.00998
2.05998
2.10999
2. 14998
2. 19990
2.24998
2.29997
2.34998
2.30998
2.42998
2.46997
2.5099B
2.54997
2.58998
2.62997
2.67998
2.71997
2.68997
2.79997
2.90997
3.01997
3.12997
3.22998
3.33998
3.43997
3.5399B
3.64998
3.7*998
3.85999
3.96997
4.07997
4.17998
4.27998
4.37997
4.46997
4.56998
4.66998
4.75996
4.85999
4.95998
5.05998
5.15997
5.25998
5.34998
5.44998
5.53998
5.61998
5.80998
5.99998
6.17998
6.35999
6.53998
6.70998
t. 90997
7.08998
7.25998
7.42998
7.60999
7.78998
7.95998
8.1299T
8.30998
8.48997
8.66998
8.84948
9.02998
9.20998
9.40997
«. 56998
9.77998
9.95998
10.13998
10.30998
10.49998
10.67998
10.83978
10.99998
484
-------
CM.CULA1ION& F(lK GRAVIMETRIC FIOH
P.IIN NO. > 198
UAIC _ .9 Ib
DRV WT." 103.10
CORRECTION* -5.10
...
-
-
TIME
(MINI
1.00
._ 2.00 _
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
11.00
12.00
13.00
..14.00 _
15.00
16.00
17.00
18.00
19.00
.. 20,00.. .. ... _
21.00
22.00
. 23.00 _
24.00
25.00
. 26.00
27.00
28.00
29..00
30.00
33.00
36.00
39.00
42.00
45.00
48.00
51.00
54.00
57.00
60.00
63.00
66.00
69.00
7J.OO
. 75.00
78.00
ni.no
84.00
87.00
90.00
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
J32.00
138.00
144.00
150.00
156.00
162.00
Ib8.00
174.00
180.00
la(>, oo
192.00
198.00
204.00
210.00
71b.OO
222.00
228.00
734.00
24,0.00
246.00
25?. 00
256*00
204.00
270.00
27b»00
782.00
2 1)1). 00
294 .00
300.00
SII2 2000. PPM
71 HO « (50. PPM
KG 02 3.% *
MB H2U ' 6.0 *
MASS DIAL
0.5100
0.5100
0.5100
0.5100
0.5100
0.5100
0.5100
J>.5100 ..
0.5100
0.5100
0.5100
0.5100
0.5100
0, 55.50 .
0.5550
0.5550
.. . __..0, 5550
0.5550
0.5550
0.55SO
0.5550
0.5550
.0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
O.SI'.O
0.5550
0.5550
0.55'jO
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5050
0.5550 _
0.5550
0.5550
0.5550
0.5550
0.5550
O.5550
0.5550
0.5550
O.S550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.4550
0.5550
0.5550
0.5550
0.5550
0.5550
0.6000
0-6000
O.bOOO
0.6000
O.bOOO
0.6000
0.6000
0.6000
O.bOOO
0.6000
O.hOOO
0.6000
0.6000
0.6000
0.6000
0.6000
p.6000
0.6000
0.6000
0. 61)00
O.hOOO
0.6400
0.6400
T6MP .
Fit)
H2SD4 >
CHART
INCHES
8.11
8.19
8.27
8.34
8.42
8.50
8.58
8.67
8.74
8.81
ft. 89
8.98
9.06
0.07
0.13
0.19
9,21
0.34
0.41
0.46
0.55
0.62
0.69
0.76
0.82
O.flS
0.97
1.03
J.JQ
1.08
1.37
-L.57
1.76
1.95
2.14
2.32
2.51
2.70
2.89
3.08
3,27._
3.46
3 '.64
. 3.82
4.01
4.20
4,40
4.59
4.79
4.99
5.18
5.38
5.58
5.77
5.97
6.18
6.39
6.69
6.80
7.01
7.47
7.84
8.25
8.67
9.06
9.49
0.89
-J.2,9
l.bB
2.08
2.48
2.89
3.30
J.71
4.11
4. SI
_ .t'1*'
5.36
5.74
*.U
6.S7
6.41
1, it
7.69
B.07
a. 45 _
8.8)
0.94
l.iO_.
1.46
200. UCC. f.
1500. CC/KIN
77.32 %
PICKUP
IMG H2S04I
1.90997
1.9B997
2.06998
2.13998
2.21999
2.29999
2.37997
2.46999
2.51998
2.60999
2.68999
2.77998
2.85999
2.86906
2.92998
2.98997
3.06998
3.13998
3.20998
3.27998
3.34998
3.41998
3.48997
3.55998
3.61998
3.68999
3.76997
3.82999
3.89998
3.87997
4.16998
4.36998
4.55998
4.74998
4.93999
5.11998
5.30998
5.49998
5.68999
5.R7997
6.06998
6.25998
6. 43999
6.61998
6.80998
6.99998
7. 19998
7.38998
7.58998
7.7B998
7.979V8
6.17998
B. 37997
8.56998
8.76997
8.97998
9.18999
9.48997
9.59998
9.80998
10.21999
10.63998
11.04999
11.46999
11.87997
12.28998 ""
12.68999
13.08998
13.47998
13.87997
14.27998
14.68999
15.09998
15.50998
15.90997
16. 10998
16.74998
17.15997
17.53998
17.9299B
I8.3199U
18.70998
19.00998
I9.4H997
19.8699*
20.24998
20.62997
20.73997
' 20.99
-------
APPENDIX A-17-3
S02 SORPTION RATES FOR DETERMINATION OF THE S02
ACTIVITY OF POST-TREATED (NH4>2S EXTRACTED CARBON
SAMPLES USING DIFFERENTIAL RATE APPARATUS
486
-------
CAICUIATIONS fllh GkAVIHtlHIL film
C-70-77 (VIRGIN)
.. .RUN NO, 180
IMH « 9 "»
tut m.. 95.10
.COSKElUllN' -6.18
. MEAN LUAU
CMS S02/100 GKS C
0.87202 ...
0.4)410
0.99B43
1.05519
1.11195
1.16871
1.22189
1.27449
1.32867
1.38543
1.44477
1.49637
1.54023.:
1.59105
1.64601
1.69761
1.74663
I. 79565
.. ...1.84725 . .
1.90142
1.96076
2. U2011. -
2.07686
2.13»M
.- 2.19030 .._.
2.24714
2.30132
2.35550
2.40968
2.51604
2.68831
, 2.85859
3.02371
3.19141
3.36168
3.52939
.. .3.69450
3.B5704
4.01958
4.18728
4.35756
4.52525
4.6B779
' 4.B5549
5. 02834
. 1 . 5.19604 . _
5.36116
5.52886
._ 5.69398 ..
5.05651
6.01905
6.16095
6.30543
6.46797
6.62534
6.78014
6.93494
7.0H974
7.24454
7.47157
7.76827
8.06239
6. 15908
8.65062
t. 93700
.9.211)21
9.4')427
9.77291
10.04331
10. 30431
10.54040
10. /K426
11.01645
11.24149
11.467'It
1 I.6H9H2
11.906S4
12.111110
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HOM S02/GM C-M1N
. _ 0.72239 .
0.61917
0.56760
0.56760
0.56760
0.56760
. .0.516O2
0.51595
0.56760
0.56760
0.61925
0.41273
0.46445
0.56760
0.51595
0.51602 ..
0.46438
0.51602
. 0.5159i_,
0.56760
0.61925
0..56760
0,56752
0.56760
..- _ 0.56760 .
0.56760
0.51602
0.56760 . ..
0.51602
0.55038
_ 0.584J9.
0.55041
0.55038
0.56760
0.56760
0.55041
0.55036
0.53319
0.55U41
0.56760
0.56760
0.55038
0.53319
0.58479
0.56760
.. ...... 0.55041
0.55038
0.56760
0. 53119
0.55041
0.53319
0.41280
0.5503B
0.53319
0.51600
0.51600
0.51600
0.51600
0.51597
0.49Bt>0
0.49020
0.49019
0.49B60
0.47300
0.4B159
0.45579
0.46440
0.46439
0.43U60
0.429V9
0.3U699
0. »95'>9
0.37H40
O.I7U40
0. I6-JM
0. I6^H()
0. «'-260
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0. 13540
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CMS ACID/100 &MS I
l.J35?B '
1.4)799
I. 52885
1.61577
1.70260
1. 71)959
1.87256
1.V5157
2.03452
. ... 2.12144 ._._
2.21231
2.29132
. _. ..2.J5B4T
2.4374'V
2.52045
2.59946
2.67452
2.74959
2.82860.
2.91155
3.00242
. ..3.0?329_. _
3.1B020
3.26710
.. . Jj 35402 _
3.44093
3.52369
3,60666
3.63982
3.B5575
4,11640.
4.3T722
4.63006
4.04684
5.14758
5.40437
5.65721
5.90609
6.1549U
6.41177 ...
6.67251
6.92930
7,17818
7.43496
7.69965
7.95644
8.20928
8.46606
B. 71890
8.9677H
9.21667
9.43396
9.65519
9.90407
10.14506
10. 38209
10.61913
10.85617
11.CV320
11.44085
11.89517
12.'34553
12.74985
13.^4626
13.69470
14.11539
14.5I8IU
14.')t>477
15.37950
15.7785'!
16.15388
16.51 tin
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17.2lt5H
17.1oO?9
17.9UU04
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1.10616
0.94810
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0.06913
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0.8691 1
0.79016
0.79004
0.86913
0.86913
0.94822
0.63199
0.7112C
0.86913
0.79004
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0.71107
0.79016
0.79004
0. 869 13
0.94822
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0.84281
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0.86913
0.84261
0.34277
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0.86913
0.84277
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0.89545
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_ 0.84281 ._.
0.84277
0.86913
0.81645
0.84281
0.81645
0.63211
0.84277
0.81645
0.79012
C. 79012
0.79012
0.79012
0.79008
0.76378
0.75062
0. 75060
0.76370
0.72428
0.7)744
0.69793
0.71112
0.71109
0.67161
0.65R4 »
0.59258
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0. 5/942
0.5/042
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0.56626
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0.31687
0.48160
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0. 69371
0.77856
0.85341
0.93077
1.01811
1.10296
1.16201
1.26266
1.34251
1..419B1
1.49971
1.57958
1.65443 . .
1.72680
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1.9)641
2.00129
2.06617
2.12607
2.18096
2.230J7
2.28078
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2.38059
2.42801
2.53780
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2.87468
3.03189
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3.336)2
3.48605
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1.93023
4.07496
4.21969
4.36442
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4.78365
4.925S9
5.04816
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5.45740
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5.73439
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6.011)6
6.14B62
6.28587
6.42312
6.55787
6.68763
6.87229
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7.39632
7.66083
7.91785
8.17238
8.42691
8.68144
8.92849
9.16804
9.40760
9.64965
9.89669
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1,54713
1.34751
0.99U14
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0.798',7
0.69870
0.84650 ..
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0.79B54
0.79854
0.79H47
0.79854
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0.51581
0.7174t.
0.91705
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2.00572
2,17418
2.29645
2.41873
2.53335
2.64416
2.75879
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2.96513
3.06448
3.16383
3.25554
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3.49244
3.568H6
3. 64528
3.7178b
3.86601
4.14966
4.40186
4.64258
4.87566
5.10875
5.33801
5.56345
5.79272
6.01116
6.23978
6.46140
6.68302
6.9008?
7.11098
7.32496
7.54276
7.72999
7.92104
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9.20492
9.41506
9.62524
9.83540
10.04173
10.24043
10.52119
10.91294
11.32561
11.71064
12.12421
12.51196
12.90370
11.29345
13.67174
14.01856
14.40539
14. 77603
15.154H
15.52876
15.89942
16.27005
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0. 47011
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0.66063
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1.03425
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1.14312
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1.30147
1.35143
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1.50189
1.54643
1.59097
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1.6H499
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1.65572
1.69283
1.92747
1.96459
2.05119
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2.29119
2.40748
2.52378
2.64007
2.75141
2.R57B1
2.96421
3.G7U6U
3.39720
3.38216
3.46628
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3.68917
3.79062
3.BB960
3.96857
4.0B754
4.27006
4.36961
4.46116
4.55518
4.64921
4.74076
4.82963
1.91690
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6.05214
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6. 564 12
6.71217
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0.31342
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2.07244
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0.75780
0.83354
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0.75780
0.68195
0.68195
0.68207
0.75769
0.68195
0.60622
0.68195
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0.60622
0.68195
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0.60618
0.58094
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0.58C94
0.55569
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2.60370
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0.53045
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0.46726
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0.45465
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0.41677
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2.03326
1.H84U
1. 04 13 7
1.73S6>
1.53139
1.48768
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1. 23978
1.23'J7S
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1.140S8
0.99161
0.991BS
0.99161
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0.94225
0.94225
0.79340
0.84304
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0.79348
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0.64304
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0.87611
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0.79345
0.79345
0.61000
0.69427
0.81000
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0.7' 389
0. 17693
0.72732
0.76041
1.057V4
0.429 It
0.727)4
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0.71002
0.7273*.
O.S9510
0. (6038
3.69427
0.67775
0.66123
0.66121
0.66121
0.66123
0.64468
0.64468
0.6446(1
0.62815
0.62816
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1. 44659
1. 14654
1.97054
2.18316
2.43375
2.66536
2.b779d
3.07541
3.26905
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3.64114
3.81199
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4.14232
4.30558
4.45746
4.60934
4.76121
4.90928
5.05356
5.18645
5.31174
5.44463
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5.02431
5.95720
6.08629
6.352C7
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7.10005
7.46454
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8. 17835
8.52386
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9.26424
9.61734
9.96660
10.31216
10.65388
11.07154
11.41324
11.679C2
12.U1694
12.35106
12.68139
12.96514
13.29647
13.63059
13.94572
14.25327
14.55702
14.86076
15.16451
15.46446
15.76061
16.05676
16.49339
17.07051
17.62865
18.16400
10.69176
19.21191
19. F2450
20.2251-8
20. 61.471
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22.406h6
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t
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3.11343
2.B8551
1.59460
2.65771
2.35413
2.27800
1.97442
1.97431
1.89841
1.B984I
1.74651
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1.59472
1.74651
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1.51882
1.51871
1.51871
1.44281
1.44281
1.21490
1.29091
1.36692
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1.21490
1.36692
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1.29091
1.34154
1.21501
1.21497
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1.24031
1.06311
1.24031
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1.21497
1.1390D
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1.11370
1.16438
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0.65810
1.U374
1.13904
1.08844
1.11374
0.91124
1.16434
1.66311
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.01247
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0.98717
0.98717
0.98717
0.961B6
0.96187
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0.82264
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0.72141
0.65810
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0.64547
0.62014
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0.54420
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(l.442'<7
490
-------
CALCULATIONS FOR GfUVlHtfHIC FLOW
R«f-7-6C-6
RUN NO. - 193
DATE 9 7 71
I>RY 1.1. 10?. 82 MG
CLRKECIION- -6.lt) MC
HtAN IUAD
CMS S02/100 CMS C
0.36777
0.49601
O.blVil
0.7)797
0.85895
0.9(509
I. 06461
1.15172
1.22)76
1.3*719
1.45659
1.55095
1.64290
1.73242
1.81464
1.89454
1. 97661
i. 05907
2.13650
2.20909
2.26409
2.35668
2.426B5
2.49460
2. 56235
2.63252
2.69543
2.7SB33 . .
2.82366
2.95190
i. 14063
3.32210
3. 49673
3.67778
3.66168
4.03831
4.21252 ..
4.39157
4.56578
4.73999
4.91178
5.08115
5.25052
5. 41990
5.62556
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6.00302
6.17723
6.34902
6. 52124
6.69261
6.86198
7.0313S
7.19589
7.35000
7.51770
7.67497
7.82982
7.9H46H
6.21444
8.51699 .__
8.79524
9.06382
9.34449 _
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9.6X690
10.15506
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10.94627
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1.25824
1.30653
1.16144
1.20980
1.20980
1.11300
0.67749
1.06463
1.01626
1,01619
0.967B.)
0.91946
0.91446
0.87110 "
0.77422
0.82273
0.82266
0.82266
0.725B5
0.725V3
0.77422
0.67749 . .
0.72593
0.62905
0.72593
0.67749
0.5B068
0.67749
0.62912
0.64522
0.61297
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0.58071
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0.61297
0.56456
0.59685
0.59663
0.56456
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0.54844
0.56071
0.54844 ....
0.58071
0.79041
0.56456
0.596*5
0.56456
0.5B071
'0.58071
0.54646
0. 58068
0.54846
0.54U44
0.53232
0.53232
0.51617
0.51619
0.51617
0.50812
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0.42746
0.46779
0.46779
0.45166
0.44360
0.44 )60
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0.41940
0.41133
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0.75951
0.94847
1.13001
1.31526
1.49310
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1.76357
1.92289
2.07850
2.23040
2.37489
2.51569
2.65277
2.77874
2.90101
3.02699
3.15296
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3.3e266
3.49752
3.60866
3.71611
3.81985
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4.03104
4.12737
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4.32374
4.52010
4.80909
5.08697
5.35743
5.63160
5.91319
6.18365
6.45042
6.72459
6.49134
. 7.25811
7.52116
7.78052
8.03987
8.29922
8.61415
8.92536
9.19213
9.45889
9.72194
9.98670
10.24806
10.50741
10.76676
11.01870
11.26694
11.51147
11.7522V
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12.22653
12.57851
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13.46772
13.87897
14. JOB76
14.73113
15.14238
15.5444*
15.95370
16.35,762
16.76147
17.154?!
17.53902
17.42114
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2.00063
1. 77845
1.85251
1.65251
1.7042B
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1.63021
1.55616
1.55604
1.48198
1.40792
1.40792
1.33386
1.18552
1.25980
1.25969
1.25969
1.11146
1.11157
1.18552
1.03740
1.11157
0.96323
1.11157
1.03740
0.88917
1.03740
0.96334
0.98799
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0.91389
0.88921
0.93662 . ..
0.93862
0.86448
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0.91389
0.06440
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0.86921
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0.88921
1.21032
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0.91393
0.1)6446
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0.88921
0.63983
0.88917
0.83983
0.83979
0.81511
0.81511
0.7903B
0.7904?
0.79036
0.77B06
0.76570
0.65455
0.71631
0.71631
0.69160
0.679/6
0.67926
0.6bf>89
0.67926
0.66691
0.64219
0.64221
0.629H5
0.04221
0.60516
0.60514
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0.542BO
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0.44141
0.54341
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491
-------
C4lCUl»IIONi Ft)« GKAVIHllKIt
IHI'tRIMtNl!,
R«T-7-lt-7
RUN Ml. 194
DAM 'I 1 71
DRY Hi." 10). JO HG
COHftfU ION* -5. 911 KG
MEAN tO/10
CMS SU2/100 CMS C
0.7)929
0.782)6
0.82781
0.87567
(<.v2)52
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1,02400
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1.12210
1.160)8
1.19627
1.23455
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1.3I82U
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1.37810
1.41876
1.45945
1.49773
1.5)601
1. 57479
1.61257
1.64846
1.68195
1.71)06 ._. .
I. 74416
1.77287
1.60398 ...
1.8)747
1.89250
1.97624
2.06237
2.14611
2.22507
2.30402
2.38298
2.45954
2.5)849
2.615C5
2.68444
2.75143
2.82081
2.89020
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3.02418
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3.15337
3.22037
3. 28497 . .
3.34717
3.409)8
1.46919
3.52901
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3.66299
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3.79219
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1.91899
4.01469
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4.37597
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4.62958
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4.99804
5. 11766
5.2)968
5.36170
5.4UI »
5.59857
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5.825H6
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DtFfeRfNIIftl RATE
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0.43064
0.43064
0.47854
0.47U47
0.47054
0.52636
0.47847
0.526)6
0.43G72
0.13492
0.362U2
0.3S2S2
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0.43064
0.19145
0.38282
0.43064
0.38282
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0.3828?
0.38274
0.38282
0.3)499
0.33492
0.2871/
0.33492
0.23927
0.38282 _
0.28709
0.27M5
0.21)712
0.28709
0.27115
0.25521
0.27115
0.25521
0.25521
0.27115
0.239^5
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0.22330
0.23927
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0.22330
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0.22330
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0.207)4
0.19142
0.20734
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0.20735
0.19938
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0.17545
0.17545
0.16740
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2.01862
2.06675
2.11022
2.17250
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2.29340
2.35202
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2.46925
2. 52420
2.575»9
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2.67075
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2.89789
3.C2612
3.15801
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3.52803
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3.76617
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4.U054
4. 21312
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4.42562
4.52820
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4.72969
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5.12536
5.22061
5.31220
5.40)79
5.50637
5.60896
5. 70768
5.60679
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6.0009A
6.14750
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6.51752
6.70070
6.89171
7.08905
7.2t>322
7.47006
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0.80600
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0.51285
0.58619
0.58619
0.65942
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492
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CALCULATION!! rim (.RJVIHICRIC HUH KPCRIMINIi
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0.489 16
0.5H292
0.66689
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1.00190
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3.60077
3.71352
3.82627
3.93902
4.05176
4.16211
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4.38262
4.50036
4. 61551
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0.95955
0.91160
0.76767
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0.71965
0.71972
0.62367
0.62374
0.62374
0.57572
0.52777
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0.52777
0.47981
0.47974
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0.36765
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0.89260
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2.53092
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2.92397
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3.05988
3.18845
3.37579
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3.74312
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4.11046
4.29045
4.47045
4.64677
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5.68632
5.85697
6.03162
6.20426
6.37324
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6.71119
6.89118
7.06750
7.23648
7.40912
7.57BIO
7.74708
7.91605
6.08502
8.25032
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8.82704
9.16111
9.49926
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10. 16047
10.4S372
10.79963
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11.42044
11.71614
12.05225
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.10207
0. 95499
0.^5511
0.95511
O.tol-,7
0.80814
0.80814
0.07343
0.80814
0.80814
0.7)472
0.73460
0.73472
0.8U814
0.73460
0.66129
0.58775 . ._..
0. 7)460
0.73472
0.66118
0.58775
0.58775
0.. 7 3460
O.D6129
0.63670
0.61223
0.6122)
0.61223
.__ 0.61223
0.61223
O.D6775
0.61223
0.56324
0.56775
.0.58771 ...
0.56324
0.58775
0.56324
0.58775
0.56)24
0.5S775
0.56324
0.56324
. 0.56327
0.56324
0.6)670
0.53676
0.58775
0.56324
0.56327
0.56324
0.56324
0.56324
0.53876
0.55100
0.55102
0.56)24
0.56)26
0.55100
0. 5)876
0.51876
0.51427
0.5142'!
0.5/650
0.526'.2
0.52650
0.5020)
0.50201
0.52650
0.51427
0.52hS2
0.50?C)
O.S020I
0.4H9/9
0.4n'l7f
0.417'.)
0.4/751
C.46MO
0.45104
0.46S30
0.440110
P. 4411 III'
C.4.'H'>7
U.4I611
493
-------
CALCUUUONS FUR GRAVIMtrHIC FLOM
a«r-7-6C-»
BUN NO. l">6 SU2 _ 2000, PPM TfMP «_ 200. PEO. f.
OAlf 9 14 71 140 « 150. PPH Fill * 1500. CC/MIN
OdY WT.- 100.42 HC 02 3.5 * H2S(K ' 75.78 *
*EAN LOAD OlFf EfUNTIAL RATS H6AH LOAD . .. DIFFERENTIAL RATE
iKS S02/100 SHS C KGM S02/GM C-MIN CMS ACID/100 CHS C MfcH ACIU/GM C-MIN
n.4tftAq O.49?R590
1.20363
1.24136
1,2790?
1.31305
1.34324
1.J7719 _..
1.41493
1.45266
1.4«662
1.52057
1.55453
1.58472
1.61490
1.64836
1.68262
1.71301
1.76582
1.84506
1.93184
2.01862
2.10163
2.18464
2.26387
2.33933
2.414UO
2.49026
._ Z..5657.3
2.64119
2.71665
2.79212
2.86758
2.94304
3.01850
3.09019
3.16188
3.23357
3.30149
3.36941
3.43732
3.50147
3.56184
3.62590
3.69012
3.75427
3.61841
3.90897
4.03725
4.17309
4^30892
4.44098
4.576BI
4.71642
4.85225
4.98809
5. 12015
5.25598
5.39182
5.92387
5.65593
5.78799
i.9238)
6.05589
6.18795
6.32001
6.44630
6.57281
t.6'1732
6.82561
6.95)89
7.07841
7.20292
.. 7.J31Z1.
7.4557?
7.50024
7.f04,T6
0.402/6
0.37734
0.45276
0.45276
0.37/34
0.45276
0.37/34
0.37734
0.45276
0.45276
0.45276
0.37734
0.37V34
0.37734
0,37722
0.30192
0.301110
0,37/34 _.
0.37734
0.37/34
0.301(10
0.37734
0.30180
0.30192
0.30189
0.37734
0.30192
0.30180
0.25156
0.27670
0.30184
0.27670
0,27670
0.27670
0.25152
0.25156
O..O156
0.25152
0.25156 _
0.25152
0.25156
0.25156
0.25152
0.25156
0.25152
0.22643
0.25152
0.22&38
0.22642
0.22638
0.22638
0.20124
0.20124
0.2263B
0.20124
0.22638
0.20124
0.20124
0.22638
0.22640
6.22638
0.21381
0.23B97
0.22640
0.72638
0.22640
0.21381
0.23897
0.21381
0.22638
0.21381
0.22640
0. 22638
0.21383
0.226)8
0.21381
0.21381
0.20U4
0.213HI
0.213HI
0.21381
0.20124
0.21381
0.21381
0.20124
0.21381
O..2012i
494
-------
CALCULATIONS FOR GRAVIMETRIC FLOW EXPERIMENTS
R»T-7-6C
RUN NO.
DATE
DRY UT.»
197 __W>2_' 200p._PPH TEMP » 200. DEC. f_.
91571 NO- 150.>PM"" Tin*1500. CC/HIN
98.30 MG 02 3.5 X H2S04 > 74.7) X
-.JltQ
MEAN LOAD
'CMS S02/100 CHS C
_PIFFERENTIALJUTE_
MGH S02/GK C-MIN
_ _M£AN LOAD
CMS ACID/100 CM$"C~
DIFFERENTIAL RATE
"MGM ACIO/CM C-MIN"
0.58831
0.61299
0.66774
0.70001
0.72980
0.76208
0.79*34
O.B2662
O.B5BB9
. ._0. 88867 .
0.92095
0.95322
. .... 0. 9830.1. _
1.01031
1.03514
.. .... 1.05748-..
1.07982
1.10464
1.15429
1.17663
1.19641.
1.21634
1.2)620
1.25606 .
1.27592
1.29578
.--1.31812
1.34046
1.36280
, .1.41742
1.47203
1.52664
.. .1.57811...
1.63090
1.68303
1.73268
1.78481
1.83694
... .- -1.88.90J _
1.94368
1.99829
2.10007
2.14972
2.24404
2.29369
2.38802
2.4)767
2.48732
2.53696
2.5B661
2.6)37B
2.68094
2. 72811
2.77031
2.83733
2.93166
).02351_
3.11287
3.20224
3.28912
3.38097
3.475)0
3.56218
3.64658
3.733'.,
).822S)
3.90971
3.99411
4.08099
4.170)6
4.25972
4.34909
4.4)845
4.5770?
4.62215
4.71648
4.80833
4.90017
4.9H954
5.0764Z
5.16579
5.25763
5.3*203
i.*Z147 ...
0.54612 0.90085 0.83625
0.34757
0.3*7*9
0.29787
0.29795
0.3*7*9
0.29787
0.34757
0.29787
0.297B7
0.34757
0.29787
p. 29787
0.24825
0.24825
0.19B56
0.24825
0.24825
_ 0.24818
0.24825
0.19B<>)
0.19846
0.19856
0.19863
3.96927 0.
t.022*B 0.
.07189 0.
.11751 0.
.16693 0.
.2163* 0.
.26575 0.
.31517 0.
.36078 0.
.41020 0.
.45962 0.
.50523 0.
.54704 0.
.58505 0.
.61926 0.
53221
53210
45612
45623
53210
45612
5)221
45612
45612
5)221
45612
45612
)801)
38013
30404
.653*7 0.38013
.69148 0.38013
.72949 0.38002
.76750 0.
.80171 0.
1.8)212 0.
38013
30*15
30404
1.8625) 0.30404
1.89294 0.30415
L. 92)35 - 0.30404
0.19863 1.95376 0.30*15
0.19856 1.98417 0.30*04
O.J4B25 2.01B37 0.38013
0.19856 2.05258 0.
0.18204 2.08679 0.
Or|R?G4 2.170*2 0.
30404
27875
27875
0.18204 2.2540* 0.27875
0.18204 2.33767 0.27875
O.16r>5Q 2.41749 0.25342
0.1B204 2.49732 0.
0.16548 2.5771* 0.
0.165SO 2.65316 0.
27875
25338
25342
O.lBiO* 2.7)299 O.iloty
0.16550 2.81281 0.25342
0.18704 2.B9264 0.27875
0.1B202 2.97626 0.
0.18204 ' 3.05988 0.
0.16550 3.13970 0.
0.16550 3.21573 0.
0.16548 3.29175 0.
0.14894 3.36397 0.
0.16550. 3.4)619 0.
0.16550 3.51222 0.
n.l<.R94 3.58444 0.
0.16550 .65666 0.
0.16548 .73268 0.
0.16550 .80870 0.
0.16548 .88472 0.
0.16550 .96075 0.
0.1489* *. 03297 0.
0.16550 4.10519 0.
0.1*B9* 4.17741 0.
0.13240 4.24203 0.
0.15722 4.34466 0.
0.15722 4.48911 0.
0.14894 4.62975 0.
0.1*895 *. 76659 0.
0.1*89* 4.90)42 0.
0.14067 5.03646 0.
0.16549 5.17710 0.
0.14895 5.32154 0.
0-14.067 5.45458 0.
0.14067 5.58383 0.
0.14895 5.71687 0.
0.14894 5.85370 0.
0.14067 5.98674 0.
0.14067 6.1I59B 0.
0.14895 6.24902 0.
0.14894 6.)8Srtft 0.
0.14895 6.52270 0.
0.14U9* 6.65954 0.
0.141195 6.79638 0.
0.14894 6.9)322 0.
0.16549 7.07766 0.
0.141195 7.22210 0.
0.15722 7.36275 0.
0,1*894. 7.50)39 0.
27871
27875
25342
25342
25338
22806
25342
25342
2J58.P.6
25342
25338
253*2
25338
253*2
22806
25)42
22B06
20273
2407*
2407*
22806
22808
22806
21539
25)40
22808
2153?
215)9
22808
22806
215)9
21539
22808
22806
22808
22806
22808
22806
25340
22808
24074
22806
0.14895 7.6*02) 0.22808
0.1*067 7.77)27 0.21539
0.15722 7.91011 0.2407*
0.14BV4 8.05075 0.
0.132*0 8.17999 0.
.__ 0.1)i40. _ 8. 30163 0.
22806
2027)
2027)
495
-------
CALCULATIONS f(JK ORAVIMETRIC FLOW EUPtRIMtNTS
C-70-77 TBfATCO HUH 2« NH4UM
HUN NO. 198 S02 2000. PPM TFMP 200. DEC. F. r
OAII: . ~9 16 'll~ NO 150. "»M FITI ' '" 1500. tC/HIN ~
DRY MT.- 103.10 MC O2 * 3.5 X H2S04 77.32 *
CO?R£CTlyN« -5.|0 KG H20 « 6.0 *
K£AN LOAp
GUI S02/100 CMS C
0.95503
<
-----
"*
-
0.99421
1.0)094
1.06763
1.10686
1.14604
1.18767
1.22665
1.2611)
1.29787 ..
1.33950
1.38113
. ..1.40316 ....
1.42031
1.44969
1.48397
1.52071
1.55499
I.5H977
1.62356
1.65784
1.692J2
1.72641
1.75824
1. 79QOB
1.82681
1.86109
-1.H9Z93.
1.97129
2.09128
2*. 1B6Z9
2.27984
2.37290
2.46350..
2.55411
2.64717
2.74022
2.83328
2.92633
3.01918..
3.10999
3.19815
3.38181
3.47731
1.57787
3.66832
3.76628
a. 86 178
3.95728
4.05523
4.15074
4.24624
4.34664
4.44950
4.57438
4.67479
4.75315
4.90498
5.10823
$.31148
5.51473
5.71790
... 5.91879
6.11714
6.31)05
. 6.50651
6.69996
6.89587
7.0942,
7.29502
7.49583
.. 1.69416 _..
7.89009
8.09579
. B. 30)94
8.49739
8.68595
_ B. 87696... _
9.06797
9.2565)
9.44754
9.63854
9.62466
J0.0107I_ _
10.11076
10.221)1
10.J4070
DIFFERENTIAL RATE
MGH S02/CH C-HIN
0.39182
0.39182
0.34287
~~ 0.39182
0.39175
0.44084
0.34280
0.34287
0.39182
0.44077
0.39182
Q..04895
0.29305
0.29)85
0.39162
0.)42B7
0.34280
0.34280
0.342B7
0. 14780
0.34287
0.29)85
0.391 />
0.29)92
0.47345
0.32650
0.31019
0.31019
0.31019
0.79185
0.31019
0.31019
0.51019
0.31016
0.31019
0.11019
0.29387
0.29385
0.11019
0.31019
0.32650
O.V1019
0.32650
0.32650.
0.31019
0.32650
0.32650
0.31019
0.32650
0.34285
0.34285
0.48974
0.17958
0.34285
0.3)468
0.3428)
0.33468
0.3428)
0.33466
0... J34.de
0.32652
0.32650
. £.3.10.15 . .
0.32650
0.32652
. . 0.33468 . ..
0.31466
0.3)468
0.32650.
0.32652
0.35416
... 0.33466
0.31019
0.31835
0.31835 , ,
0.31815
0.31019
0.31019
0.31019
0.11018
0.08979
0.21224
. .D.llZil ..
MEAN LOAD
CMS AC ID/ 100 CMS C
1.46239
1.52238
1.57863
1 .63488
1.69488
1.75487
1.81862
1.87861
1.93111
1.98736
2.05110
2.11485
2.14860
2.17484
2.21984
2. 27233. _
2.32858
2.38108
2.4)358
2.48607
2.53857
2.59107
2.64356
2.692)1
2.74106
2.797)0
2.84980
2.89855
3.01854
3.20228
3.49101
3.63350
3.77224
3.91098
4.05347
4.19597
4.33845
4.48094
4.62343
4.76218
4.89716
5.03590
5.17840
5.32464
5.47088
5.61712
5.76711
5.91334
6.05959
6.20957
6.35581
6.50206
6.65580
6.81329
7.00453
7.15827
7.27826
7.51075
7.82198
8.13321
8.44444
8.75566
9.06314
9.36688
9.66686
9.96309
10.259)1
10.55929
10.6630)
11.17050
11.47798
.11.78171
12.08170
12.39666
.12.71541
13.0116)
13.300)7
13.5928*
13.8853)
14.1 7406
. 14.46654
14.74902
15.04401
15.12899
15.51272
15.65147
15.84645
DIFFERENTIAL RATE
MCH AC10/CM C-MIN
0.59997
0.59997
0.52502
0.59997
0.59997"
0.59986
0.67504
0.52491
O. 52502
0.59997
0.67493
0.59997
0.07495
0.44995
0.44995
0.59997
0.52502
0.52491
Q. 52502
0.52491
0.52502
0.52491
0.52502
0.44995
0.52502
0.59986
0.45007
0.52491
0.72497
0.49996
Q.47497
0.47497
0.47497
0.44995
0.47497
0.47497
0.47497
0.47494
0.47497
0.47497
0.44999
0.44995
0.47497
0.47497
0.49996
0.47497
0.49996
0.49996
0.47497
0.49996
0.49996
0.47497
0.49996
0.52498
0.52498
0.74992
0.27498
0.52498
0.51247
0.52496
0.51247
O. 52496
0.51245
0.51247
0.49998
0.49996
0.48747
0.49996
0.49998
0.5124?
0.51245
0.51247
0-49996 __
0.49498
O.S4997
0.51245
0.47497
0.48747
0.46747
0.48747
0.47497
0.44996
0.47497
0.4749T
0.47496
0.1)749
0.32499
0.324*1
496
-------
APPENDIX A-18
LITERATURE STUDY ON SOLVENT EXTRACTION
A literature survey on the removal of sulfur from carbon" by
extraction was made.
The paper by Prchlik, et al.14 was of particular interest.
The paper discussed a detailed study based on both literature
and experimental work of sulfur extraction from spent gas
works purification mass (iron oxide). Literature references
on 10 solvent systems for sulfur extraction from spent purifi-
cation mass were given. Solubility data for sulfur in various
solvents were given. These data are shown in the following
section. Diagrams of bench scale extraction apparatus and
proposed commercial equipment are given. In reviewing various
solvents and running bench scale tests, Prchlik, et al. reached
the following conclusions:
1) Carbon disulfide, while an excellent solvent, is
discounted due to the-health and explosion hazards
inherent in its handling.
2) Chlorinated solvents, trichloroethylene and dichloro-
benzene, were discounted primarily due to cost
although it was also mentioned that trichloroethylene
will not remove the pitch or naphthalene present in
the gas being treated.
3) Tetralin was considered an excellent solvent but was
discounted because of expense and difficulty in
removing it from the purification mass.
4) A toluene-xylene mixture was considered the best
solvent in view of the requirement to remove pitch
and naphthalene as well as sulfur to regenerate the
purification mass.
Ammonium sulfide was not considered by the authors, presumably
because of its reactivity with the iron oxide.
Equilibrium Data - Sulfur-Solvent Systems
Solubility of Sulfur in Ammonium Sulfide
No extensive data on the solubility of sulfur in ammonium
sulfide was found. Previous extraction processes operated
near room temperature and under these conditions the solubility
was reported to be 18-2470 by weight of sulfur in solution14'15.
Since the pressure of H2S and NH3 were important for extraction
studies at higher temperatures these data are shown in
Tables A-1B-1 and A-18-2 and Figure A-18-1.
497
-------
Table A-18-1.
VAPOR PRESSURES OF H2S, NH3, AND H20
OVER AQUEOUS (NH4)2S SOLUTIONS
Temp . ,
°C
20
20
20
20
20
40
40
40
40
60
60
60
60
NH3,
% by Wt.
1.38
2.68
6.77
8.05
9.41
2.31
5.88
7.21
9.34
3.22
5.54
6.80
9.00
H2S,
% by Wt.
1.40
2.68
6.81
8.03
9.40
2.33
5.86
7.26
9.36
3.25
5.56
6.81
9.05
Vapor Pressure, mm. Hg
H2S
53.3
65.6
130.1
154 . 8
190.0
92.0
183.4
220.5
293.2
134.1
205.0
250 . 9
365.0
NH3
0
0
0
5.6
13.0
8.2
22.2
26.9
30.4
25.5
48.5
76.1
145.0
H20
16.3
16.2
15.8
15.1
14.3
49.1
44.7
48.4
47.9
125.1
127.3
113.5
105.0
Table A-18-2.
VAPOR PRESSURES OF H2S, NH3, AND H20
OVER AQUEOUS (NH4)2HS SOLUTIONS
Temp . ,
°C
20
20
NH3,
% by Wt.
0.80
2.14
2.97
H2S,
% by Wt.
1.58
4.23
5.93
Vapor Pressure, mm. Hg
H2S
115.7
163.0
197.6
NH3
0
0
0
H20
13.9
15.2
16.1
498
-------
Figure A-18-1.
1000
Equilibrium vapor pressures of hydrogen
sulfide and ammonia over aqueous
ammonia solutions at 20°C
Hydrogen Sumde
2.On
l.On
0.5
0
0.2 0.4 0.6 0.8
Mole H7S/Mole NH (R)
£ O
499
-------
Solubility of Sulfur in Carbon Disulfide
The solubility of sulfur in carbon disulfide is strongly
dependent upon temperature, reaching 9070 at 98°C. Data from
the literature on solubility are contained in Table A-18-3 .
Table A-18-3.
SOLUBILITY OF SULFUR IN
CARBON DISULFIDE
Temp. ,
°F
-110
-100
-90
-80
-70
-60
-50
-40
-30
-20
-10
% Sulfur
in Solution
1.0
1.5
2.0
2.5
3.2
4.2
5.5
7.1
9.5
12.0
15.0
Temp . ,
°F
0
10
20
30
40
50
60
70
80
90
98
7o Sulfur
in Solution
19.0
23.5
30.0
38.5
50.0
60.0
66.0
71.0
78.5
86.0
90.1
Solubility of Sulfur in Xylene
The solubility of sulfur in meta and para-xylene is up to
21.8% in solution is shown in Table A-18-416. There is no
solid phase of sulfur in equilibrium with the solution above
21.8% and a liquid-liquid separation occurred. There was
500
-------
Table A-18-4. SOLUBILITY OF SULFUR IN XYLENE
m-Xylene
Temp.. °C % Sulfur in Solution
25 1.969
45 3.604
80 10.29
Rhombic Sulfur-p-Xylene
% Sulfur in Solution Equilibrium Temp. , °C
11.0 85.0
13.95 92.5
17.85 100.5
Monoclinic Sulfur-p-Xylene
% Sulfur in Solution Equilibrium Temp., °C
16.25 98.2
16.3 98.0
17.85 103.3
20.38 106.0
21.8 107.0
apparently the formation of amorphous sulfur. Table A-18-5
gives the solubility results before measurable amounts of
amorphous sulfur were formed.
These data indicate that sulfur and p-xylene are initially
mixcible in all proportions above about 190°C. However, if
the equilibrium temperature is maintained, reseparation of
liquid phases occurs, probably due to the formation of
501
-------
Table A-18-5.
SOLUBILITY OF SULFUR IN p-XYLENE ABOVE
21% CONCENTRATIONS BEFORE PHASE
SEPARATION
% Sulfur
in Solution
20.38
21.8
25.9
27.95
28.04
30.22
31.95
34.6
34.9
39.9
44.0
Equilibrium
Temp . , °C
94.0
101.0
117.7
124.5
124.2
130.0
137.3
144.5
149.0
158.5
167.0
% Sulfur
in Solution
44.1
45.7
46.3
48.3
61.7
71.2
81.0
85.6
87.9 .
90.0
91.0
Equilibrium
Temp . , °C
167.5
171.0
175.0
175.0
190.0
190.0
184.0
176.0
162.5
150.0
143.0
amorphous sulfur, resulting in a rise in the temperature
of complete miscibility. The equilibrium temperatures
finally obtained are contained in Table A-18-6.
Table A-18-6.
SOLUBILITY OF SULFUR IN p-XYLENE
AT ELEVATED TEMPERATURES
70 Sulfur
in Solution
16.25
21.8
25.9
27.8
27.95
29.1
30.22
31.95
34.6
34.9
36.0
Equilibrium
Temp . , °C
80
109.0
121.7
127.0
129.0
132.0
133.7
141.5
148.25
150.0
154.0
70 Sulfur
in Solution
39.9
44.0
44.1
45.7
46.3
48.3
87.9
90.0
91.0
96.2
Equilibrium
Temp. ,°C
165.0
174.5
174.5
179.5
183.5
196.0
177.0
155.0
147.5
84.0
502
-------
The equilibrium temperature rises with sulfur concentration
below 48.3/o and decreases with sulfur concentration above
87.9/0. There does not appear to be a maximum, however. Rather
the low and high concentration curves appear to be entirely
separate. The temperatures above which two phases exist and
below which one phase exists are:
S in Solution, Equilibrium Temp.,
44.0
46.3
48.3
87.9
90.0
91.0
235.0
220.0
206.0
187.0
203.0
205.0
Smisek and Cerney17 also present data on the solubility of
sulfur in xylene as shown in Table A-18-7. These data agree
rather well with the literature information in previous tables
Table A-18-7.
SOLUBILITY OF SULFUR
IN XYLENE
Temperature,
°C
25
45
85
100
107
Concentration ,
Wt. %
1.73
3.24
10.78
18.8
24.1
503
-------
The following equilibrium data as presented in Prchlik's
article!^ are referenced to the original author:
System: Sulfur-Benzene18
Temp . , °
25
54
84
C g. S/100 g. Sat
2.074
5.165
13.02
. Soln.
System: Sulfur -Toluene
Soln.
Temp . ,
OF
-10
0
0
13
15.5
20
23
25
35
40
50
54
60
70
80
83.5
90
100
Dissolved g. of S
in 100 g. of
Sat. Solns .
0.576
0.923
0.897
1.545
1.649
1.827
1.889
2.018
2.722
2.35
3.68
4.85
5.27
7.83
11.1
11.64
15.3
20.9
Determined By
Jacek19
Jacek19
Hildebrand-Jenks 18
Delaplace20
Jacek19
Delaplace20
Delaplace20
Hildebrand-Jenks 18
Hildebrand-Jenks L 8
Burden-Newling 2 !
Burden-Newling
Hildebrand-Jenks 18
Bur den - Newl ing 2 ^
Bur den - Newl ing
Bur den- Newl ing2 ^
Hildebrand-Jenks l 8
Bur den-Newl ing "
Bur den - Newl ing 2 1
System: Sulfur-p-Xylene22
Temp . , °
85
92.5
98.0
100.5
107.0
117-121
124-129
C g. S/100 g. Sat.
11.9
13.95
16.3
17.85
21.8
25.9
27.95
Soln.
504
-------
Bituminous
Pitch Oil Fraction
Temp . B . P .
°C S.G.
15
30
50
80
100
110
120
130
, °C: 80-100
: .87
2.1
3.0
5.2
11.8
15.2
85-120
.88
2.3
4.0
6.1
13.7
18.7
23.0
27.0
120-220
.882
2.5
5.3
8.3
15.2
23.0
26.2
32.0
38.7
i i
Coal)zz
by Boiling Point
150-200
.885
2.6
5.8
8.7
21.0
26.4
31.0
38.0
43.8
210-300
1.01
6.0
8.5
10.0
37.0
52.5
105.0
Range
220-300
1.02
7.0
8.5
12.0
41.0
54.0
115.0
505
-------
APPENDIX A-19
DETAILED DATA FROM COMBINED SULFUR STRIPPING/H2S
GENERATION STUDIES
Page
1. Run SHG-1 507
2. Run SHG-2 512
3. Run SHG-3 517
4. Run SHG-5 522
5. Run SHG-7 527
6. Run SHG-8 532
7. Run SHG-9 537
8. Run SHG-10 542
9. Run SHG-11 548
506
-------
RUN SHG-1
A. EXPERIMENTAL DATA - IJ2.S GENERATION/S STRIPPING
1. Virgin Carbon
a. % Sulfur (Combustion Anal.), Psc
2. Inlet Carbon -
a. %, Sulfur (Combustion Anal.), Psi
b. Acid Titration, Pvi
c. Material Rate, RI
7.
= 0.65%
= 20.70%
= 40.6 Ibs./hr.
Intermediate
a. Stage 8,
b. Stage 7,
Stage 6,
Stage 5,
Stage 4,
Stage 3,
Stage'2,
Stage 1,
c
d
e
f
g
h
Stage Carbon
% Sulfur, PS8
% Sulfur, PS7
% Sulfur, Ps6
% Sulfur, PS5
% Sulfur, PS4
% Sulfur, Ps3
% Sulfur, PS2
% Sulfur,
Outlet Carbon
a. %, Sulfur (Combustion Anal.), Pso
b. Material Rate, R0
/
Inlet Gas
a. % H2 (26.0% by Rota)
b. H2 Gas Rate (55% @ 4.3 PSI)
c. N2 Gas Rate (25.8% of 640 @ 4.3 PSI)
Intermediate Stage Gas Analysis
H2S % N2 % SO2 % H20
15.79%
37.3 Ibs./hr.
26.8 Chrom. %
66 CFH @ 70°F
188 CFH @ 70°F
% CO % CO2
1
2
3
*j
4
^r
5
«/
6
\*'
7
Outle
a.
b.
c .
d.
e.
f .
g-
h.
7°
10
01
lo
7
10
7
to
7
lo
7
10
21.4
4.1
21.8
1.3
18.1
16.0
15.8
0
0
2
0
6
6
8
t Gas Analys
H2
H?S
N2
SO?
H20
CO
CO?
Sulfur
(as
.88
.96
.0
.2
.4
is
si)
72
70
71
91
71
71
71
.0
.4
.7
.1
.9
.4
.0
i
0
0.3
0
0
0
0
0
0.08
0.56
0
0
0.14
0.49
0.90
=
=
=
0
0
0
0
0
0
0
1 ^
16
4
68
6
1
f^ nt
.27o
1%
.3%
f\ Of
.2/0
.3%
f\m
n i
* \J fo
S7
. ~> lo
0.04
0.05
0.04
0.04
0.04
0.05
0.10
507
-------
8.
Temperature
Stage Carbon/Gas, °F
1
2
3
4
Stage Carbon/Gas,°F
768/800
111/
781/800
778/
5
6
7
8
801/806
799/
---/801
734/
9.
Cyclone Product
a. Sulfur =
b. Material Rate =
c. 7o Material +40 Mesh
d. % Material -40 Mesh
B. SULFUR MATERIAL BALANCE, SULFUR REMOVAL, AND H2S CONVERSION
1. Run Start
3
4,
5.
6.
7.
8.
9.
10.
11.
12.
13.
Run Times
Run Time
Steady State Period
Inlet Carbon Analysis
Outlet Carbon Analysis
Inlet Sulfur Loading,
Outlet Sulfur Loading, PSQ
Inlet Material Rale, Rsi
Outlet Material Rate, RSo
Cyclone Sulfur Loading, P
-1680-1690
1680-1890
1720-1890
1647-1817 (-73 tnin)
1776-1946 (+56 rain)
20.70%
15.79%
40.6 Ibs./hr.
37.3 Ibs./hr.
scy
Cyclone Material Rate, RSCy = 0.0055 Ibs./hr.
Gas Rate In, qT = 254 CFH @ 70°F
N2 Rate In, q^2 = 188 CFH @ 70°F
H2 Cone. In, 100
112 Cone. Out, 100
H2S Cone. Out, 100
S02 Cone. Out, 100 ygo
1120 Cone. Out., 100 (yH2o)o
CO Cone. Out, 100 YcOo
C02 Cone. Out, 100 (vr)
" ^
Sulfur Vapor Out, RSVO
O
negligible
in balance
508
-------
GAS AND CftRBON rLOW RATES
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COLUMN TEMPERATURES. PRESSURES, AND PRESSURE
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RUN SHG-2
A EXPERIMENTAL DATA - H2S GENERATION/S STRIPPING
1. Virgin Carbon
a. % Sulfur (Combustion Anal.), PSC =
2. Inlet Carbon - Precursor C-72-108 - Act. (0.598)(10~3)
a. % Sulfur (Combustion Anal.), Psi = 20.31%
b. Acid Titration, Pv£ -
c. Material Rate, Ri =35.1 Ibs./hr
3. Intermediate Stage Carbon
a. Stage 8, % Sulfur, Ps3
b.
c .
d.
e .
f.
g-
h.
Stage
Stage-
Stage
Stage
Stage
Stage
Stage
7,
6,
5,
4,
3,
2,
1,
7
/o
7
/o
7
/o
7
/o
7
/o
7
/o
7
/o
Sulfur,
Sulfur,
Sulfur,
Sulfur,
Sulfur,
Sulfur,
Sulfur,
PS7
PS 6
PS 5
PS4
PS3
PS2
PSI
4. Outlet Carbon
a. % Sulfur (Combustion Anal.), Pso = 4.85%
b. Material Rate, Ro =29.1 Ibs./hr.
5. Inlet Gas
a. % H2 (29.3% by Rotameter) = 32.0 Chrom. %
b. H2 Gas Rate (57 RRx1.1 FF = 3 PSI) = 67 CFH @ 70°F
c. N2 Gas Rate (41% of 360 @ 3 PSI) - 162 CFH @ 70°F
6. Intermediate Stage Gas Analysis
Stage % H2 %Jt2_S % N2 % SO2 % H20 % CO % CQ2
0.1 0.52 0 0
00 00
0 0.25 0 0
00 00
0 0.41 0 0.05
0 0.61 0 0.1
7.
10.0%
6S'.570
8.5%
0
1.25%
5.5%
512
1
2
3
4
5
6
7
Outle
a .
b.
c .
d.
e .
f .
g-
h.
/o
%
%
to
7
/o
%
%
%
t Ga
"2
H?.S
N2
SOy
H20
CO
C02
7.
24.
24.
21.
13.
10.
8
7
2
5
0
3
s Analy
Sulfur
(as
0
0
1.
4.
6.
16.
sis
-
0
4
1
9
73.3
72.8
74.3
74.6
71.2
73.3
SD
-------
8. Temperature
Stage Carbon/Gas, OF
1 942/997
2 970/
3 982/997
4 967/
9. Cyclone Product
a. Sulfur
b. Material Rate
c. % Material +40 Mesh
d. % Material -40 Mesh
Stage Carbon/Gas,°F
5
6
7
8
1001/997
970/
7970
840/
= 3131 (Start
B SULFUR MATERIAL BALANCE, SULFUR REMOVAL, AND H2S CONVERSION
1
3
4
5
6
7
8
9
10
11
12
13
Run Start
Run Times
a. Run Time
b. Steady State Period
c. Inlet Carbon Analysis
d. Outlet Carbon Analysis
Inlet Sulfur Loading, Psi
Outlet Sulfur Loading, PSo
Inlet Material Rate, Rsi
Outlet Material Rate, RSO
Cyclone Sulfur Loading, P
3131 (Started C at
Feeder +95 min)
3226-3408
3262-3408
3167-3313
3326-3472
20 . 31%
4.85%
35.1 Ibs./hr.
29.1 Ibs./hr.
(+36)
(-95)+36
(+64)+36
scy
%
°
;./hrj
Cyclone Material Rate, Rscy = 0.0033 Ibs
= 162 CFH @ 70°F
= 32.0 vol. %
negligible
Gas Rate In,
N2 Rate In,
H2 Cone. In, 100
H2 Cone. Out, 100
100
Out,
Out, 100 yso
Out, 100
Out, 100
Out, 100
H2S Cone
S02 Cone
1120 Cone
CO Cone.
C02 Cone
Sulfur Vapor Out, RSvo
513
-------
Ss
33 ai-
GAS AND CARBON FLOW RATES
TYP£
NO.
H',tt. Pr^ss.
De.-jsit;/; 3-5
- Prccsure at Outlet, cf ?.ol&=eter Read at N2 Hotaacter Outlet; App. - Ga.-. F.'ov
6 - K2 Ficv for Lever Carton Seal Leg; LTA-101 - Ng Flow for Upper Carbon Se> 1 :
C4TE |c
!
> FP? 7? I
it-e, l«o Correction;
*?-Pi£N3..;8?.,fVN
Cor^ - Gas Flow Pate Correct*
RSAD AND UN7r^STOO'D !
^ x. A4J / ii/vb !
i i
-------
GAS ANALYSIS
4" OIA. REGENERATOR
RUN NO. S^g- 2.
PEED
DATE
T!-
AN")
-------
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Ul
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r.9055 REFERENCES;
1BD
II^HtllVilVi^i'^*-1
1 ftZ - C,:**?:'* a* -e --c f.'.'-i: -:: c":.-<-~.l ' i
;
i
kn qp
1 ! : ! ! i i ill 1
1 i i i 1 i i
0 aog.rn',To:~p<: 1i« 'i5« cii |»i» rc"C> -!«- ;?>! "rf ire' 1 «>»»' 'to i ' ' <"»a
J 1
s icftrr
V.
t.o| | ^'^
S-4!
5
^,
^
.
i
l»:-.
'.:
1
at(j/j
^
r
1 ! i ! ! - 1 !i i i
I : i . i iii i '
?Jo I'll ;?'"! »7"'/r'- 7' -J5" .^tr '?>: ''~o »:'?:'-' «<.-. ' «-"^"c7^i ! '/j?7
y^-^rn i rj V ! 77-^ J7-U- i j ^ 1 ! i
J ! .
'ft-. i??o We ?/!.'
~7
(
F*-"
^
i
1
raturvi.
L'zjf.a.j&i
V7o ni5 :*y1o
1 . 1 ! ! i :
1 i 1 1 , i . - 1 jli';!
fcf&'iTf £Vc'f7o ff> {c-s/se*1;?* &'-,-: '.r- T/:'- ' HV i--" ' ' ' "VJo
?9"'?A2J S5J /a,-r'-H- .r~J./c«>";«j !f.o "."?:- 'W1 1 ?5>' ^^ '' ' i = ^^ I
(iiitaMi ISSP-IcSJ'?'!-''^ ^c 'Sw :?r Emit.
-------
RUN SHG-3
A. EXPERIMENTAL DATA - H2S GENERATION/S STRIPPING
1. Virgin Carbon
a. 7o Sulfur (Combustion Anal.), PSC
2. Inlet Carbon -
a. 7. Sulfur (Combustion Anal.), Psi = 20.35%
b. Acid Titration, Pv± =
c. Material Rate, R± =30.9 Ibs./hr.
3. Intermediate Stage Carbon
a. Stage 8, 7. Sulfur, Ps8
b. Stage 7, 70 Sulfur, PS 7
c. Stage 6, 7o Sulfur, P$6
d. Stage 5, 7» Sulfur, PSS
e. Stage 4, 7. Sulfur, PS4
f. Stage 3, 7> Sulfur, Ps3 =
g. Stage 2, 7o Sulfur, Ps2
h. Stage 1, 7. Sulfur, PSI
4. Outlet Carbon
a. 7o Sulfur (Combustion Anal.), Pso = 2.8270
b. Material Rate, Ro =23.85 Ibs./hr.
5. Inlet Gas
a 70 H2 (27.2% by Rotameter) = 29.870
b H2 Gas Rate (4570 Scale, Assume 1.1 PSI) = 52 CFH @ 70°F
c. N2 Gas Rate -