EPA-600/2-76-135b
May 1976
Environmental Protection Technology Series
                 DEVELOPMENT OF THE WESTVACO
                 ACTIVATED  CARBON  PROCESS  FOR
           SOX  RECOVERY AS ELEMENTAL SULFUR
                              Volume I - Appendix
                               Industrial Environmental Research Laboratory
                                    Office of Research and Development
                                   U.S. Environmental Protection Agency
                              Research Triangle Park, North Carolina 27711

-------
               RESEARCH REPORTING SERIES

Research reports of the Office of Research and Development, U.S. Environmental
Protection  Agency, have been grouped into five series. These five broad
categories were established to facilitate further development and application of
environmental technology. Elimination of traditional grouping was consciously
planned to foster technology transfer and a maximum interface in related fields.
The five series are:

     1.    Environmental Health Effects Research
     2.    Environmental Protection Technology
     3.    Ecological Research
     4.    Environmental Monitoring
     5.    Socioeconomic Environmental Studies

This report has been  assigned  to the ENVIRONMENTAL  PROTECTION
TECHNOLOGY series. This series describes research performed to develop and
demonstrate instrumentation, equipment, and methodology to repair or prevent
environmental degradation from point and non-point sources of pollution. This
work provides the new  or  improved technology required for the control and
treatment of pollution sources to meet environmental quality standards.
                    EPA REVIEW NOTICE

This report has been reviewed by  the U.S.  Environmental
Protection Agency, and approved for publication.  Approval
does not signify that the contents necessarily reflect the
views and policy of the Agency, nor does mention of trade
names or commercial products constitute endorsement or
recommendation for use.
This document is available to the public through the National Technical Informa-
tion Service, Springfield, Virginia 22161.

-------
                                         EPA-600/2-76-135b

                                         May 1976


      DEVELOPMENT OF THE WESTVACO

         ACTIVATED  CARBON PROCESS

FOR  SOX RECOVERY AS ELEMENTAL SULFUR

              VOLUME  II--APPENDIX
                          by

     G. Nelson Brown, Carl M. Reed, Albert J. Repik,
       Robert L. Stallings,  and Samuel L. Torrence

                       Westvaco
                       Box 5207
         North Charleston,  South Carolina 29406
                Contract No. 68-02-0003
                 ROAPNo. 21ACX-085
              Program Element No. 1AB013


        EPA Project Officer: Douglas A. Kemnitz

       Industrial Environmental Research Laboratory
         Office of Energy,  Minerals, and Industry
           Research Triangle Park, NC  27711


                     Prepared for

      U.S. ENVIRONMENTAL PROTECTION AGENCY
           Office of Research and Development
                 Washington, DC 20460

-------
                       TABLE OF CONTENTS
Section                                                     Page
 A        DETAILED RAW DATA AND DATA ANALYSIS                 1
 A-l         Experimental Results of Gravimetric Flow         2
               Experiments
 A-2         Computer Calculations - Sorption Rate Data      26
               and Models
 A-3         Comparison of Westvaco Model to Experimental    52
               Sorption Data
 A-4         S02 Sorption Rate Studies in 1" Diameter        79
               Fixed Bed
 A-5         SO? Sorption Studies in 6" Diameter Fluid       83
               Adsorber
 A-6         Multiple Regression Analyses                    95
 A-7         Comparison of Multiple Regressions to           99
               Differential Rate Data
 A-8         Comparison of Multiple Regressions to 6"       120
               Diameter Fluidized Bed Runs
 A-9         S02 Sorber Design - Effects on Size            142
 A-10        Reaction Rate Studies for Sulfur Generation    224
               in 1" Diameter Fixed Bed
 A-ll        Sulfur Generation Experimental Data            238
 A-12        Detailed Results of Integral Runs              247
 A-13        Data from Solvent Extraction Experiments       378
 A-14        Literature Survey for Recovery of Sulfur       388
               by Solvent Extraction
 A-15        S02 Activity and Pore Volume Determination     398
               of Solvent Extracted Carbon
 A-16        Experimental Results of Bench Scale Recycle    435
               Tests - Solvent Extraction versus Hydrogen
               Treatment
 A-17        Post-Treatment Results of Ammonium Sulfide     471
               Solvent Extracted Carbon
 A-18        Literature Study on Solvent Extraction         497
 A-19        Detailed Data from Combined Sulfur             506
               Stripping/H2S Generation Studies
 A-20        Derivations                                    553
                               ill

-------
Section                                                    Page
 A-21        Sample Calculations for Integral Testing       605
 A-22        Computer Programs                              613
 A-23        Detailed SC>2 Sorber Data Analysis              650

 B        DETAILED PILOT PLANT INFORMATION                  664
 B-l         Analytical Techniques                          665
 B-2         Integral Pilot Plant Operation                 697
 B-3         Blueprints                                     706
 B-4         Pilot Plant Operating Manual                   726
 B-5         Safety Program for Pilot Plant Operation of    789
               Westvaco Process

 C        DETAILS OF PROCESS COMMERCIALIZATION              815
 C-l         1,000 MW Utility Boiler Flue Gas Clean-up,     816
               Detailed Economic Evaluation
 C-2         15 MW Detailed Equipment Design and Cost       825
                              iv

-------
             APPENDIX



            SECTION A



DETAILED RAW DATA AND DATA ANALYSIS

-------
                       APPENDIX A-l



EXPERIMENTAL RESULTS OF THE GRAVIMETRIC FLOW EXPERIMENTS

-------
                GRAVIMETRIC    FLOW   EXPERIMENTS
Run:          138 . G
Dry Weight:   97.30 mg.
Deflection:   -10.80 mg.
C02:          H.3%
S0:          2000 ppm
NO:
02:
H20:
t:
150 ppm
0.7%
10%
200°F
% H2S04:     72.51
Correction:  0.4735
Date:        April 21, 1971
Ft:   1000 cc/min.
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
189
190
200
210
220
230
240
250
260
270
280
290
300
306
Load
mg. H2S04/g- C
3.39
5.65
7.09
8.22
9.35
10.28
11.00
11.72
12.44
13.16
14.59
15.93
17.37
18.71
20.04
23.23
26.62
'29.80
32.79
35.87
38.85
41.73
44.60
47.48
50.36
53.13
55.91
58.58
61.36
63.93
66.60
71.84
76.88
81.71
86.43
90.96
95.79
100.62
105.55
110.79
116.03
121.07
126.10
131.14
136.28
141.32
146.25
151.18
156.22
161.25
166.08
168.96
Mean Load
mg. H2$04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160














•





Rate
mg. H2S04/g. C/min.
3.3402
2.4152
1.6958
1.1614
0.8530
0.72Q7
0.6989
0.6783
0.6680
0.6578
0.6372
0.6269
0.6064
0.5858
0.5755
0.5653
0.5498
0.5396
0.5344
0.5242
0.5190
0.5139
0.5087
0.5087
n.5036
0.5036
0.4985
0.4933
0.4882
0.4882
0 . 4882
0.4830





















-------
GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
C02:
S02:
139
101.30 mg
-9.83 mg.
11.335
2000 ppm
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
Load
mg. H2S04/g. C
9.28
11.65
13.33
14.61
15.89
17.08
18.26
19.15
20.14
21.13
23.10
25.17
27.15
29.22
31.29
36.43
41.46
46.50
51.33
56.17
61.01
65.75
70.58
75.22
79.86
84.70
89.34
93.98
98.72
103.26
107.90
116.98
126.26
135.44
144.52
153.50
162.29
170.48
178.58
186.57
194.18
201.88
209.28
216.78
224.09
231.29
238.30
245.21
252.02
258.64
264.46
                 NO:
                 02:
                 H20:

                 Ft:
150 ppm
2.0%
10.0%
200° F
1000 cc/min.
% H2S04--     73.58
Correction:  0.4805
Date:        April 22,
1971
Mean Load
mg. H2S04/q- C
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240
260













* Rate
mg. H2S04/g. C/min.
9.5953
6.9497
5.1135
2 . 8924
.7473
.4610
.2833
.1846
.1155
.0464
.0365
.0168
1.0069
0.9970
0.9872
0.9773
0.9674
0.9576
0.9526
0.9427
0.9378
0.9329
0.9279
0.9230
0.9181
0.9082
0.8983
0.8885
0.8786
0.8638
0.8490
0.8342
0.8193
0.7996
0.7848
0.7453
0.7108
0.6663














-------
                GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
G02:
S02:
140
99.86 mg.
-9.78 mg.
11.3*
2500 ppm
NO:
02:
H20:
t:
Ft:
150 ppm
2.0%
10.02!
200° F
1000 cc/min.
% H2S04:
Correction:
Date:
 72.91
 0.4761
'April 23, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
i 230 .
240
246
Load
mg. H2S04/g. C
6.91
9.11
11.02
12.42
13.92
15.22
16.52
17.82
19.03
20.23
22.63
25.14
27.54
29.84
32.04
37.65
43.16
48.47
53.68
58.88
64.09
69.20
74.20
79.31
84.42
89.33
94.23
99.34
104.45
109.25
114.06
123.77
133.29
142.60
151.71
160.73
169.34
177.65
185.66
193.47
201.38
209.29
216.90
225.72
233.83
238.03
Mean Load
mg. H2S04/g. C
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
220
240









Rate
mg. H2S04/g. C/min.
6.2588
4.5063
2.1330
1.7725
1.5522
1.4070
1.3219
1.2568
1.2217
1.1566
1.1316
1.1166
1.1015
1.0865
1.0765
1.0665
1.0565
1.0465
1 .0365
1.0314
1.0214
1.0114
1.0064
0.9964
0.9914
0.9764
0.9563
0.9463
0.9363
0.9213
0.9063
0.8862
0.8712
0.8512
0.8362
0.7961
0.7561










-------
               GRAVIMETRIC   FLOW    EXPERIMENTS
Run:
Dry Weight:
Deflection:
C02:
502=
141
100.50 mg.
-11.35 mg.
11.3%
1500 ppm
NO:
02:
H20:
t:
Ft:
150 ppm
2.0%
10.0%
200 °F
1000 cc/min.
% H2S04:     74.01
Correction:  0.4834
Date:        April 26, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
230
"240
250
260
270
280
290
300
310
320
330
340
350
360
366
Load
mg. H2S04/g. C
6.07
8.36
9.75
10.85
11.94
12.94
13.83
14.83
15.82
16.82
18.81
20.80
22.79
24.78
26.77
31.64
36.52
41.39
45.97
50.35
54.73
59.00
63.18
67.46
71.64
75.62
79.70
83.78
87.96
92.04
96.12
104.08
111.94
119.70
127.36
134.83
142.69
150.25
157.31
164.68
171.74
178.61
185.37
192.24
199.00
205.47-
211.64
217.61
223.38
228.96
234.33
239.10
243.98
248.46
253.23
257.91
262.29
264.78
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
220
240
260









'









Rate
mg. HgSO^g. C/min.
6.9154
5.7015
3.1343
1.5423
1.2637
1.1294
1.0597
1.0149
0.9950
0.9800
0.9751
0.9602
0.9502
0.9403
0.9254
0.9154
0.9055
0.8955
0.8856
0.8756
0.8706
0.8657
0.8557
0.8458
0.8408
0.8308
0.8159
0.8010
0.7861
0 . 7662
0.7463
0.7214
0.7015
0.6766
0.6517
0.6269
0.5721
0.5224
0.4627




















-------
GRAVIMETRIC   FLOW   EXPERIMENTS
Run:          142
Dry Weight:   99.18mg.
Deflection:   -11.64 mg.
C02:          11.3*
S02:
                 NO:
                 02:
                 H20:
                 t:
150 ppm
2.0%
10.01
200° F
1 H2S04:     71.88
Correction:  0.4694
Date:        April 27, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
?80
290
300
310
312
Load
mg. H2S04/g. C
6.25
7.66
9.07
10.18
11.39
12.60
13.61
14.62
15.63
16.54
18.25
19.96
21.78
23.59
25.41
29.74
34.08
38.31
42.75
46.98
51.02
55.05
59.08
63.12
67.05
71.08
74.71
78.34
82.17
85.80
89.53
96.69
104.36
112.12
119.78
127.24
134.70
142.06
149.22
156.48
163.44
170-30
176.95
183.10
189.66
196.01
202.16
208.11
214.16
220.00
225.45
230.59
231.50
                 Ff.    1000 cc/min.
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190.
200
220
240















Rate
mg. H2S04/g. C/min;
7.0075
5.1220
2.9744
1.3410
1.1595
1.0536
0.9831
0.9377
0.9125
0.9074
0.8923
0.8822
0.8671
0.8570
0.8469
0.8369
0.8268
0.8167
0.8066
0.8016
0.7915
0.7814
0.7764
0.7663
0.7562
0.7512
0.7360
0.7209
0.7058
0.6907
0.6755
0.6604
0.6453
0.6251
0.6050
0.5848
0.5445
0.5041
















-------
                GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
C02:
S02:
143
100.02 mg.
-12.38
11.3%
500 ppm
NO:
02 :
H20:
t:
150 ppm
2.0%
10.0%
200 °F
1000 cc/m1n.
Correction:
Date:
72.45
0.4732
April 28, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
340
350
360
370
380
390
400
410
420
Load
mq. H2S04/Q. C
4.50
6.10
7.40
8.50
9.50
10.50
11.40
12.00
12.90
13.60
15.00
16.50
18.00
19.40
20.70
24.00
27.09
30.29
33.49
36.59
39.59
42.49
45.39
48.39
51.19
53.99
56.59
59.59
62.49
65.39
68.09
73.49
78.88
84.18
89.48
94.68
100.08
105.78
111.18
116.68
122.08
127.37
132.47
137.87
142.97
148.17
153.47
158.77
163.97
169.07
173.77
177.86
182.26
186.46
190.66
194.96
198.76
203.56
208.16
212.66
217.06
221.56
225.75
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220


























Rate
mg. H2S04/q. C/min.
4.6491
2.9794
1.4497
1.1498
0.9648
0.8498
0.7698
0.7199
0.6849
0.6649
0.6549
0.6399
0.6299
0.6249
0.6149
0.6049
0.5999
0.5949
0.5849
0.5799
0.5749
0.5699
0.5649
0.5599
0.5549
0.5499
0.5449
0.5349
0.5249
0.5149
0.5049
0.4949
0.4799
0.4699
0.4599
0.4449
0.4149

•



















V



•

-------
                GRAVIMETRIC   FLOW   EXPERIMENTS
Run:          144 -  G
Dry Weight:   98.68  mg.
Deflection:   -10.07 mg.
C02:          11'3%
503:          2000 ppm
NO:
02:
t:
Ft:
150 ppm
3.5%
10.0%
200°F
1000 cc/m1n.
% H2S04:     73.31
Correction:  0.4788
Date:        April 29, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
Load
mg. H2S04/g. C
7.60
10.03
12.16
14.09
15.91
17.73
19.36
20.98
22.50
24.12
27.16
30.20
33.14
36.08
38.91
46.01
53.10
60.09
67.09
73.98
80.97
87.86
94.65
101.34
108.23
115.02
122.11
129.00
135.79
142.48
149.07
162.04
174.40
186.46
198.52
209.97
221.02
231.96
242.30
252.23
261.96
271.08
279.89
288.61
297.02
Mean Load
mg. H2S04/g. C
4
6
8
10
12
14
16
18
20
25
30
35
40
. 45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240
260
280






Rate
mg. H2$04/g. C/min.
7.2963
5.1176
3.4455
2.1078
1.9457
1.8494
1.7734
1.7075
1.6417
1.5505
1.4998
1.4745
1.4593
1.4491
1.4390
1.4289
1.4187
1.4086
1.3985
1.3934
1.3883
1.3833
1.3731
1 . 3681
1 . 3630
1.3529
1.3427
1.3326
1.3174
1.2971
1.2819
1.2566
1.2262
1.1958
1.1654
1.0995
1.0336
0.9627
0.8918







-------
                GRAVIMETRIC   FLOW   EXPERIMENTS
Run:         145 . G
Dry Weight:  100.90 mg.
Deflection:  -2.31 mg.
S02:         2000 ppm
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
Load
mg. H2S04/g. C
8.92
11.40
12.98
14.47
15.86
17.24
18.53
19.92
21.31
22.70
25.27
27.85
30.33
• 33.00
35.48
41.13
46.78
52.43
57.88
63.43
68.78
74.23
79.68
84.94
90.19
95.34
100.59
105.65
110.80
115.76
120.91
130.92
140.63
150.05
159.27
168.29
177.01
185.53
194.15
202.48
210.51
217.84
224.98
232.31
238.85
NO:   150 ppm
02:   2.0%
H20:  10.0%
t:    200°F
Ft:   1000 cc/min.
% H2S04:     72.61
Correction:  0.4742
Date:        April 30, 1971
Mean Load
mg. H2S04/g. C
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
' 60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240








Rate
mg. H2S04/g. C/min.
8.9197
7.0862
5.2032
3.6670
2.0317
1.4668
1.4073
1.3677
1.3380
1.2834
1.2438
1.2141
1.1893
1.1645
1.1447
1.1298
1.1150
1.1001
1.0902
1.0803
1.0704
1.0605
1.0505
1.0406
1.0357
1.0208
1.0010
0.9812
0.9613
0.9316
0.9118
0.8821
0.8573
0.8Z7fi
0.7978
0.7384
0.6739








                                             1.0

-------
              GRAVIMETRIC    FLOW   EXP-ERIMENTS
Run:          148-6
Dry Weight:   100.94 mg.
Deflection:   -9.02 mg.
C02:          11.»
$03:          2500 ppm
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
Load
mg. H2S04/g. C
26.25
36.95
44.09
50.53
56.07
61.72
66.48
71.23
75.69
80.15
88.07
95.80
103.53
"110.86
117.79
133.94
1 48. 70
162.47
176.02
188.83
200.52
211.12
221.02
229.54
237.07
244.11
250.94
257.58
264.22
270.85
277.29
290.07
301.76
312.17
321.28
329.80
338.02
346.05
353.68
360.11
366.55
372.70
378.64
384.29
389.14
NO:   150 ppm
02:   2.0%
H20:  10.0%
t:    150°F
Ft:   1000 cc/min.
% H2S04:     57-18
Correction:  0.3734
Date:        May 7, 1971
Mean Load
mg. H2S04/g. C
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
. 55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
220
240
260
280
300
320
340
360
380

Rate
mg. H2S04/g. C/min.
37.9433
34.9713
32.2469
29.8197
27.4916
25.3121
23.2812
21.3989
19.6156
15.3061
11.7396
8.9657
7.2816
6.6475
6.1423
5.6965
5.3002
4.9534
4.7058
4.4977
4.3293
4.1708
4.0222
3.8934
3.7745
3.5566
3.3386
3.1405
2.9622
2.7937
2.6352
2.4866
2.3281
2.1785
2.0408
1.7832
1.5554
1.3572
1.1888
1.0402
0.9015
0.7628
0.6*39
0.5350

                                            11

-------
                GRAVIMETRIC   FLOW   EXPERIMENTS
Run:         149 -  G
Dry Weight:   105.38 mg.
Deflection:   -10.58 mg.
C02:         11.32
502'         1500 ppm
NO:   150 ppm
02:   2.0%
H20:  10.0%
t:    150°F
Ft:   1000 cc/min.
% H2S04:     56.86
Correction:  0.3713
Date:        May 10, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
210
220
230
240
Load
mg. H2S04/g. C
24.10
34.07
40.71
46.02
50.67
55.04
58.74
62.26
65.57
68.80
74.97
• 81.04
86.73
92.33
98.03
112.36
126.21
138.64
150.31
161.32
171.95
182.29
192.16
201.46
210.48
218.92
226.80
234.39
241.41
248.05
254.22
266.18
276.81
286.68
296.17
305.37
313.53
320.74
327.67
334.03
339.91
345.61
351.11
356.33
361.17
Mean Load
mg. H2S04/g. C
10
12
14
16
18
20
25
30
35
40
45
50
55
60
" 65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240
260
280
300
320
340
360





Rate
mg. H2S04/g. C/min.
26.5705
24.1032
21.8258
19.7381
17.9351
16.2744
12.5261
9.6318
7.4492
6.1207
5.1243
4.5549
3.8622
3.5586
3.3488
3.2027
3.0888
3.0129
2.9512
2.8895
2.8326
2.7757
2.6665
2.5622
2.4673
2.3771
2.2965
2.2016
2.1067
2.nilR
1.9121
1.8077
1.5942
1 . 3855
1.1909
1.0154
0.8541
0.7117
0.5883
0.4R87





                                              12

-------
               GRAVIMETRIC   FLOW   EX P. ERIMENTS
Run:          150 - 6
Dry Weight:   105.66 mg.
Deflection:   -11.50 mg.
C02:          ll.W
S02:          500 ppm
NO:
02:
H20:
t:
Ft:
150 ppm
2.0%
10.03
150°F
1000 cc/min.
% H2S04:     53.33
Correction:  0.3482
Date:        May 11, 1971
Time
mi nutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
1*0
130
140
150
160
170
180
190
200
210
220
230
240
Load
mg. H2S04/g. C
22.43
29.34
33.50
37.01
40.22
42.97
45.33
47.51
49.69
51.68
55.74
59.53
63.13
67.01
70.89
80.54
90.48
99.75
109.12
118.40
127.67
136.66
145.37
153.98
161.93
169.60
177.17
184.46
191.56
198.37
205.09
218.44
231.40
243.61
254.31
264.05
273.33
282.23
290.93
299.36
307.50
314.78
321.79
327.84
332.95
Mean Load
mg. H2S04/g. C
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240
260
280
300
320
340





Rate
mg. H2S04/g. C/min.
30.3805
24.7965
21.0581
17. .9349
15.2849
13.0134
11.0733
7.3822
5.0161
3.5018
2.7447
2.2714
2.0963
.9544 .
.8976
.8739
.8455
.8361
.8171
.7982
.7793
.7651
1.7462
1.7083
1.6846
1.6373
1.5947
1.5569
1.5190
1.4717
1.4291
1.3913
1 . 3439
1.2493
1.1546
1.0411
0.9275
0.7855
0.6388
0.4921





                                           13

-------
               GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
C02:
151 - G
101.36 mg.
-11.68 mg.
11.3%
2500 ppm
NO:  150 ppm
02:  2.0%
H20: 10.0*
t:   300°F
Ft:  1000 cc/min.
* H2S04:     81.86
Correction:  0.5346
Date:        May 12, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
340
350
357
Load
mg. H2S04/g. C
3.55
5.82
7.40
8.88
10.26
11.35
12.43
13.42
14.31
15.19
16.77
18.35
19.83
21.21
22.59
26.05
29.20
32.16
35.22
38.18
41.04
44.00
46.86
49.72
52.58
55.35
58.11
60.87
63.73
66.50
69.16
74.59
80.01
85.24
90.37
95.50
100.63
105.47
109.91
114.34
118.49
122.93
127.17
131.12
134.96
138.61
142.27
145.92
149.37
152.92
156.37
160.12
163.77
167.32
170.78
174.03
176.20
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180























Rate
mg. H2S04/g. C/min.
3.5221
2.5355
1 . 7856
1.3319
1.1247
0.9866
0 . 8879
0.8139
0.7597
0.7202
0.6511
0.6166
. 0.5919
0.5821
0.5722
0.5673
0.5624
0.5574
0.5476
0.5426
0.5328
0.5229
0.5130
0.5032
0.4982
0.4834
0.4637
0.4440
0.4242
0.4045
0.3798
0.3552
0.3256
0.3009























                                             14

-------
GRAVIMETRIC    FLO
          EXPERIMENTS
Run:         152 - G
Dry Weight:   105.94 mg.
Deflection:   -12.67 mg.
CO?:         11.»
S02:         1500 ppm
                 NO:
                 02:
                 H20:
                 t:
150 ppm
2.0%
10.0%
300°F
1000 cc/min.
* H2S04:     82.66
Correction:  0.5398
Date:        May 14, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
lo
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
'75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
310
320
330
340
350
360
370
380
390
400
420
440
4fiO
480
500
520
" 	 510 "
560
5RO
600
Load
mg. H2S04/g. C
1.32
2.27
3.02
3.87
4.63
5.29
5.95
6.51
7.17
7.83
9.06
10.19
11.33
12.37
13.50
16.05
18.50
20.77
23.13
25.39
27.75
30.02
32.19
34.36
36.44
38.32
40.31
42.19
44.08
45.88
47.67
51.16
54.56
57.67
60.79
63.72
66.74
69.85
72.78
75.61
78.72
81.74
84.58
87.60
90.52
93.35
96.00
98.36
100.72
102.98
105.44
108.08
110.44
112.80
115.16
117.61
119.78
122.05
124.22
126.39
128.56
132.81
136.87
141.02
145.18
149.05
152.92
156. 8" ft
IBoTSB 	
164.24
167.64
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
IP
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160







































Rate
mg. H2.S04/g. C/min.
0.8873
0.7363
0.6796
0.613fi
0.5758
0.5175
0.5192
0.6003
0.4861
0.1720
0.4436
0.1200
0.3965
0.377fi
0.3K34
0.3493
0.3304
0.3lfi2
0.3068
0.2Q73
0.2P79
0.2785
0.2690
0.2643
0.2549
0.2454
0.2360
0.2265
0.2171
0.2077
0.1935
0.1R41







































                   15

-------
                 GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
C02:
S02:
153 - G
103.18 mg.
-8.23 mg.
-8.50 mg.
11.3*
2500 ppm
                                   NO:
                                   02:
                                   H20:
                                   t:
150 ppm
2.0%
10.0%
150°F
1000 cc/min.
Correction:
Date:
61.24
0.3999
May 18, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
22
24
26
28
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
2lO
220
230
240
250
260
270
280
i?90
300
Load
mg. H2S04/g. C
25.10
32.86
37.89
42.55
46.62
50.01
53.60
57.08
60.28
63.58
66.87
69.88
72.79
76.08
77.99
81.99
85.00
88.00
91.01
93.91
99.73
105.25
110.87
116.59
122.12
135.39
148.19
160.50
172.13
183.76
194.90
205.27
215.45
225.24
234.54
243.26
251.60
259.45
266.91
281.06
294.44
306.55
317.60
327.39
337.18
346.48
354.91
362.47
369.45
376.33
382.73
388.64
394.46
399.79
404.83
409.48
413.94
41S.49
422.76
Mean Load
mg. H2S04/g. C
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
220
240
260
280
300
320
340
360
380
400
420
440
460
480
500
520
540
560









Rate
mg. H2S04/g. C/min.
29.0754
26.0709
23.0665
20.4497
17.9298
15.7007
10.9517
7.1719
5.5728
4.5067
4.0124
3.6763
3.3727
3.2855
3.2080
3.1401
3.0771
3.0238
2.9705
2.9269
2.8785
2.8397
2.7719
2.7040
2.6362
2.5683 .
2.4908
2.4230
2.3454
2.2582
2.1807
2.1031
1.9287
1.7639
1.5895
1.4150
1.2309
1.0467
0.8820
0.7463
0.6203
0.5330
0.4652
0.4071
0.3683
0.3392
0.3101
0.2714
0.2520
0.2326









* Run 153 - G continued on next page.
                                               16

-------
               GRAVIMETRIC   FLOW   EXPERIMENTS
(CONTINUED FROM PREVIOUS PAGE)
Run:
Dry Weight:
Deflection:
CO,
S02
153 - G
103. 18 mg
-8.23 mg.
-8.50 mg.
11.3%
2500 ppm
Time
Minutes
310
320
330
340
350
360
~ 370
380
390
400
410
420
430
440
450
460
470
480
490
500
510
520
530
540
550
560
570
580
590
600
610
620
630
640
650
660
670
680
690
700
710
720
730
740
750
Load
mg. HjSO/i/g. C
427.02
431.29
435.26
439.23
443.01
446.60
450.47
454.16
458.03
461.91
465.69
469.28
473.06
476.74
480.42
484.01
487.50
- 490.89
494.18
497.29
500.29
503.20
506.11
508. 82
511.73
514.54
517.25
519.97
522. 58
525.20
527.82
530.43
532.86
536.34
539.45
542.64
545.65
548.46
551.17
553.89
556.50
559.12
561.45
563.68
565.61
                                NO:
                                02:
                                H20:
                                t:
                                Ft:
150 ppm
2.0%
10.0%
150°F
1000 cc/min.
% H2S04:    61.24
Correction: 0.3999
Date:       May 18,  1971
                                             17

-------
               GRAVIMETRIC    FLOW   EXPERIMENTS
Run:         157 -  Q
Dry Weight:   104.66 mg.
Deflection:   -10.56 mg.
C02:         11.3%
SO?:         2000 ppm
Time
mi nutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
Load
mg. H2$04/g. C
7.93
10.13
12.04
13.85
15.77
17.39
19.11
20.64
22.36
23.98
27.33
30.48
33.73
36.98
40.13
47.96
55.80
63.54
71.47
79.02
86.28
99.08
110.93
122.59
134.15
145.61
157.18
168.26
179.06
189.66
199.98
210.11
219.85
229.51
238.87
248. 33
257.60
266 .67
275.37
283.87
291.99
299.92
306.99
313.97
320.56
326.96
NO:
02:
H20:
t:
150 ppm
2.0%
15.0%
200° F
1000 cc/min.
% H2S04:     67.91
Correction:  0.4435
Date:        May 31, 1971
Mean Load
mg. H2S04/g. C
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240
260
280
300
320





Rate
mg. H2S04/g. C/min.
7.6916
5.7806
3.7264
2.1020
.9014
.8154
.7581
.7103
.6816
.6339
.6243
.6148
.6052
.5861
.5765
.5574 •
.5383
.5288
.5192
.5001
1.4905
1.4714
1.4523
1.4428
1.4237
1 . 3854
.3472
.3090
.2708
.2326
.1943
.1561
.1179
.0892
.0606
.0128
0.9555
0.8886
0.8122
0.7357
0.6593


.


                                           18

-------
             GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Height:
Deflection:
COo:
S02:
158 - G
104.96 mg.
-14.86 mg.
11. 3%
500 ppm
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
220
240
260
280
300
320
340
360
380
400
420
440
460
480
500
520
540
B60
580
600
Load
mg. H2S04/g- C
0.86
1.62
2.29
2.95
3.53
4.19
4.67
5.24
5.72
6.19
7.15
8.00
8.86
9.72
10.58
12.39
14.10
15.82
17.53
19.25
20.87
24.20
27.34
• 30.49
33.35
35.82
38.21
40.49
42.78
44.87
47.07
48.97
50.69
52.50
54.21
55.93
59.26
62.50
65.74
68.98
72.12
75.27
78.70
82.13
85.46
88.61
91.65
94.61
97.47
100.23
102.80
105.28
107.76
no. 14
112.42
114.52
                               NO:
                               02:
                               H20:
                               t:
150 ppm
2.0%
10.0%
300°F
1000 cc/min.
% HZS04:     77.62
Correction:  0.5069
Date:        June 1, 1971
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190





















Rate
mg. H2S04/0. C/min.
0.6955
0.5526
0.4735
0.4373
0.4097
0.3859
0.3659
0.3478
0.3325
0.3173
0.2877
0.2639
0.2439
0.2287
0.2144
0.2020
0.1915
0.1820
0.1734
0.1667
0.1601
0.1543
0.1496
0.1448
0.1401
0.1353
0.1277
0.1191
0.1124
0.1058
0.0991
0.0934
0.0877
0.0819
0.07R2





















Run 158 - G continued on next page.
                                          19

-------
GRAVIMETRIC   FLOW   EXPERIMENTS
(CONTINUED  FROM PREVIOUS PAGE)
             158  - G
             104.96 mg.
             -14.86 ing.
             11.3%
Run:
Dry Weight
Deflection
S02:
Time
minutes
620
640
660
680
700
720
740
760
780
800
820
840
860
880
900
920
940
960
980
1000
1020
1040
1060
1080
1100
1120
1140
1160
1180
1200
1220
1240
1260
1280
1300
1320
1340
1360
1380
1400
1420
1440
1460
1480
1500
500 ppm.
Load
mg. H2S04/g. C
116.71
118. 9T
121.23
123.43
125.76
128.14
130.53
132.81
135.19
137.67
139.96
142.15
144.44
146.53
148.53
150.25
152.06
153.87
155.58
157.39
159.20
160.92
162.54
164.35
166.06
167.87
169.59
171.30
173.02
174.83
176.64
178.45
180.07
181.69
183.21
184.93
186.64
188.17
189.60
191.03
192.55
194.07
195.50
196.93
198.36
NO:
02:
H20:
t:
Ft:
                        150 ppm
                        2.0%
                        10.0%
                        300°F
                        1000 cc/min.
% H2S04:
Correction:
Date:
77.62
0.5069
June 1 , 1971
                             20

-------
               GRAVIMETRIC   FLOW   EXP-ERIMENTS
Run:          160 - G
Dry Weight:   102.06  ing.
Deflection:   -11.12  mg.
0)2:          H.3%
SOg:          2000 ppm
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
Load
mg. H2S04/g. C
4.90
7.15
8.82
10.09
11.66
12.93
14.11
15.09
16.07
16.95
18.62
20.09
21.56
22.93
24.20
27.53
30.57
33.71
36.65
39.58
42.52
48.30
53.69
58.50
62.81
67.51
72.11
76.72
81.32
85.83
90.05
94.16
98.47
102.88
107.39
111.70
116.30
120.91
125.51
130.41
135.31
140.60
145.89
150.99
155.50
159.12
NO:
02:
H20:
t:
150 ppm
2.Q%
5.0%
200°F
1000 cc/min.
             80.42
Correction:  0.5252
Date:        June 9, 1971
Mean Load
mg. H2S04/g. C
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160















Rate
mg. H£S04/g. C/min.
3.8017
2.6749
1.8910
1.3717
1.1660
1.0288
0.9112
0.8328
0.7643
0.6663
0.6271
0.6075
0.5R79
0.5683
0.5585 .
0.5389
0.5291
0.5193
0.5095
0.4997
0.4801
0.4703
0.4654
0.4605
0.4507
0.4409
0.4311
0.4213
0.4164
0.4115
0.4115















                                            21

-------
               GRAVIMETRIC   FLOW   EXPERIMENTS
Run:         161  - G
Dry Height:   99.64 mg.
Deflection:   -9.76 mg.
C02-         11-3%
SOg:         2000 ppm
Time
mi nutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
Load
mg. H2S04/g. C
8.03
10.44
12.24
13,95
15.25
16.66
17.96
19.07
20.27
21.48
23.69
25.99
28.20
30.31
32.52
37.64
42.65
47.47
52.29
57.21
61.92
71.36
80.89
89.82
98.25
106.78
115.11
123.44
131.67
139.90
148.03
156.76
165.19
173.73
182.06
189.88
197.61
205.14
212.57
219.69
226.62
233.04
239.46
245.58
251.91
257.53
NO:   300 ppm
02:   2.0%
H20:  10.0%
t:    200°F
F:   1000 cc/min.
% H2S04:     73.03
Correction:  0.4769
Date:        June 10, 1971
Mean Load
mg. H2S04/g. C
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
no
120
130
140
150
160
170
180
190
200
220
240
260








Rate
mg. H2S04/g. C/rrrin.
8.1794
5.8711
4.2152
2.7098
.7061
.4352
.2947
.1943
.1542
.1040
.0739
.0438
.0337
1.0136
0.9936
0.9835
0.9635
0.9534
0.9534
0.9434
0.9434
0.9334
0.9334
0.9233
0.9133
0.9033
O.R932
0.8731
0.8531
0.8430
0.8230
0.8029
0.7828
0.7627
0.7326
0.6724
0.6122
0.5420








                                           22

-------
              GRAVIMETRIC    FLOW   EXPERIMENTS
Run:          162  - G
Dry Weight:   103.02 mg.
Deflection:   -11.12 mg.
CO?:          11.S
$02:          2000 ppm
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
Load
mg. H2S04/g. C
7.86
10.10
12.13
14.17
16.50
18.83
20.97
23.30
25.72
28.05
32.91
37.86
42.90
' 48.05
53.39
67.95
82.99
97.65
112.70
128.13
143.27
171.23
197.15
222.29
246.36
267.81
286.06
302.08
316.06
329.16
341.10
351.19
360.61
369.83
378.57
387.11
395.46
403.32
411.09
417.88
423.90
429.04
434.09
438.75
443.89
448.46
NO:
02:
H20:
t:
0 ppm
2.0%
10.0*
200°F
1000 cc/min.
* H2S04:     74.59
Correction:  0.4871
Date:        June 11, 1971
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
no
120
130
140
150
160
170
180
190
200
220
240
260
280
300
320
340
360
380
400
420
440



Rate
mg. H2S04/g. C/min.
9.3671
7.8626
6.2124
4.0769
2.3685
2.1355
2.0967
2.1161
2.1646
2.2035
2.3199
2.4170
2.5044
2.5723
2.6403
2.7082
2.8053
2.8926
2.9509
2.9897
3.0188
3.0188
2.9994
2.9703
2.9412
2.8829
2.8344
2.7762
2.7179
2.6500
2.5723
2.4073
2.2326
2.0384
1 . 8443
1.6502
1.4366
1.2134
1.0289
0.8639
0.7183
0.5824
0.4950



                                           23

-------
               GRAVIMETRIC    FLOW   EXP-ERIMENTS
Run:         163 -  G
Dry Weight:   99.18 mg.
Deflection:   -11.15 mg.
C02:         H.3%
S02:         2000 ppm
Time
mi nutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290
300
Load
mg. H2S04/g. C
4.13
6.96
9.07
11.09
12.81
14.32
15.83
17.24
18.75
20.17
23.09
25.71
28.43
30.95
33.37
39.42
45.27
51.02
56.77
62.92
68.76
80.66
91.95
103.35
114.44
125.13
135.41
145.59
155.88
165.86
175.54
185.32
194.60
203.67
212.04
219.80
227.47
234.62
241.78
248.94
255.80
262.25
268.60
274.85
280.80
286.55
NO:
02:
H20:
t:
50 ppm
2.0%
10.0%
200 °F
1000 cc/min.
% H2S04:     73.33
Correction:  0.4789
Date:        June 14, 1971
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240
260
280






Rate
mg. H2S04/g. C/min.
4.1641
3.4281
2.7929
2.2686
1.8653
1.7141
1.6132
1.5326
1.4620
1.4116
1.3107
1.2603
1.2402
1.2301
1.2099
1.1998
1.194ft
1.1898
1.1847
1.1797
1.1696
1.1595
1.1494
1.1393
1.1343
1.1192
1.0990
1.0788
1.0486
1.0284
0.9982
0.9780
0.9478
0.9276
0.8974
0.8671
0.8066
0.7461
0.6755
0.6050






                                           24

-------
               GRAVIMETRIC    FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
CO?:
S02:
164 - G
98.02 mg.
-12.73 mg.
11.3%
150 ppm
NO:
02:
H20:
t:
Time
minutes
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
160
170
180
190
200
210
220
230
240
250
260
270
280
290.
300
310
320
330
340
350
360
370
380
390
Load
mg. H2S04/g. C
2.75
4.49
5.71
6.73
7.65
8.57
9.49
10.41
11.32
12.24
13.87
15.61
17.24
18.87
20.40
24.48
28.26
31.93
35.50
39.07
42.54
49.38
56.01
62.74
69.68
76.41
83.55
90.29
97.33
104.06
110.49
117.53
124.26
130.99
137.42
143.95
150.38
156.70
163.23
169.46
175.88
182.11
187.82
194.35
200.37
206.18
212.20
217.91
223.73
229.44
235.16
240.87
246.38
251.79
257.09
150 ppm
2.0%
10.0%
200°F
1000 cc/min.
Correction:
Date:
73.10
0.4774
June 15, 1971
Mean Load
mg. H2S04/g. C
2
4
6
8
10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
160
170
180
190
200
220
240

















Rate
mg. H2S04/g. C/min.
2.4791
1.7139
1.1120
0.9692
0.8988
0.8468
0.8264
0.8060
0.7856
0.7754
0.7447
0.7345
0.7141
0.7039
0.6937
0.6886
0.6886
0.6835
0.6835
0.6835
0.6835
0.6835
0.6835
0.6835
0.6835
0.6835
0.6733
0.6631
0.6631
0.6529
0.6427
0.6376
0.6325
0.6223
0.6121
0.5917
0.5713
0.5407

















                                            25

-------
                            APPENDIX
                                             A-2
 COMPUTER CALCULATIONS  -  SORPTION RATE DATA AND MODELS
CARBON C - 71   23

JUlN  MlKlilK =   1 '10 - G
I | Ml- 1 RATUKl -  200.  Ul ;",
                             21  71
TllAL  M-CIW RAIT  =  1000.0 CC/MI'I

I'M iU".l:iJf  C(!2 •-    11.3
IM ,.;U ".(   L2 -=     0. 7
PI .•'.U-.Nl'  1120 =    1 0.0

CU'JC.r.'-lTKAT H)N S02  =  2000.0  I1!'?--
CC \:Cl"J KAI [UN1  ,\f.)  •-   100.0  PPV
rM.'0

        O.OOOoO
                          RAFI-,  tiMS
          00 y,v>
          OHB7()
          0 1. 0 1 'j
          Ul U-0
          01 10'.)
          01't'jO
          018 I i
       0.0,:'! 7!)
       0.02900

       0.03620
       0.0 1'} (if.
       O.O'i.lO]
       0.0', /13
       C.00076
       0.0'>'i3h
       O.OOiiOl
       0.06 I6J
          C t> 0 2 6
          06'I'J'J
          0/20 I
       0
       0
       0
       0
       0
       0
       0. li)P>l
       0. 11876
       O.I I 602
        ,01! 70 1
        .09'i,'6
                                        0. 002'. 2
                                        0.00] 7-j
                                        O.OU123
                                        O.OOlJFi'V
                                        0.00062
                                        0. HOU').}
                                        0.0000 I
                                        O.OOO'.V
                                          , OOO'ib
                                          . OOO'io
                                          .000^6
                                          00()''«2
                                          00' >'• "-1
                                          00040
                                          CJCOj-J
                                          OU01-;
                                          0003 9266
                                    26

-------
                         Carbon,- C - 71 —
                           ^\ MU.v?ER  =   1/39   "  "
                           Tc"P£«ATim- =  200.  DEG F

                          ' U:TAL
                                    C2
                                            11.3
                                             2.0"
                                            10.0
                                     1D\' SG2  =  2000.0 PPM
                                     ICN   NO  =   150.0 PPM
PE~CE:.T H2S04
SAT'jk-TEO  LCA'
                                             73.58
                                                  0.38 GKS  H2SU4/GK C
Ni
O.C0294
0-00441
O.C0589
O.CCV36
O.COS33
O.OiC30
0.01177
0.01324
0.01^72
0.01339
0.02207
0.:-2575
0.03311
O.C3679
C. 040 47 J •.•'.
O.C5151
C.'.'.SIS
O.C5336
O.C6254
C.C6622
0.06990
0.07353
C.C3C94
C. COB 30
C. 09565
C. 10301
C. 11037
0.11773
0.12509
0.13930 '.
• 0.16138
C. 17659
C . 1 9 1 3 1
RATE, GMS H2S04/GM C-KIN
0-00706
O.Q0511
0,00376 .
O.CC213 . ;;-:
0-00129 .-••..'• • '•••..
0.00108
0.00094
0.00087
:• C. 0003 2
• . 0.00077
0.00076
0.00075
0. 00074
0.00073
: - 0.00073
- •. .^./••. ••• -. 0.00072
.."•, : • 0.00071
0.00070
0.00070
0.00069
0.00069 ...:. -•
0.00069 •:'!'•'.!:'?. £
0.00068 **'•'••"
0.00066
0.00068
0.00067
0.00066
0.00065
0.00065
0.00064
0.00062
0.00061
i .: - .. 0.00060 :.'-.
'"":. ''•;'• • 0.00059 •!/ :
0.00058
C. 00055
0.00052
t. 00049
                                                                                          KESTVACO
                                                                                          -4.94551
                                                               -5.56706
                                                               -6. 13291
                                                               -6.63297
                                                               -6.80795
                                                               -6.93355
                                                              _-7. 00967
                                                               -7 ".06 57 5
                                                               -7.11958
MCDweSTVACO
    -4.93773
_ -5.25248
    -"5.55145"
    -6. 11336
    -6.50946
    -6.7J047"
    -6.90213
                                                                                          7.12772
                                                                                          7. 12TC6
                                                                                         -7. 12561
                                                                                         -7.12491
                                                                                          7. 12420
                                                                                          7. 12336
                                                                                          7.11746
                                                                                          j. 1166';
                                                                                          7. 11047
                                                                                          7. 10413
                                                                                          7 . 09790
                                                                                          7.09140
                                                                                          7.0S479
    _.
   -7-02626
   -7.06996
   -7.05901
   -7 '.05754
   -7.04*44
 __-7. 03522
   -7.02378
   -7.01230
   -7.00070_
  ~-i.95Se5
   -6.97131
                                                                               -6.92435
                                                                               -6.90641
                                                                              ~''
                                                                                         -7.05737"
                                                                                         -7.04279
                                                                                         -_7._02773
                                                                                         -7.01735
                                                                                         -7.00746
                                                                                         :6... 99659
                                                                                         -6.9853?"
                                                                                         -6.97949
                                                                                         r£..96706.
                                                                                         -6.9534l""
                                                                                         -6.93C96
                                                                              -6.S6957
                                                                              76_vp3180
                                                                               6. H 2 94
                                                                               6.75232
                                                                               6.67473
                                                                               6.63667
                                                                               6-55679
                                                                               6.52073
                                                                               6. 39;! 31
                                                                               6.30600
                                                                               6.22046
    AMUNDSQN
    3.33011"
    2.55679
 _____ 1.88126
  ""1.064 I i"
    0.64233
    0.53750
    0.47213"
    0 . 4 J ? B I
 _____ 0.4l_0 i9_
    C . 3ti'-9 /
    0.31133
 ____ O.i7408
  ~0.37C44"
    0.3661)0
 __ 0.36319
    6.":i"5Y55
    0 . 3 S 5 -U
 ____  0.35230
    0.33046""
    0. 34682
_..0.3_4_502 _
    0.34321
    0.34137
_ _  0.33057
    0.3? 77 7 ""~
    0.33413
____ 0...3 3.0.43 _
    0.32683
    C. 32324
_ Q. 3 177.9 _
   6.3"l2~35
   0.30690 .
__ C..J01/.2_
   0.29417
   0.23873
                                                                                                                                 0.26150
                                                                                                                                 0.24513

-------
                        RU
       '  139

.  0^3 M2S04/GM
 O.CC683
 0-J"857
 O.C'J98l_  __
 0.0-1075
 O.CU69
 0.01257
                                                  4 22 71

                                                       JOST^

                                                    0-'-6663
                                                    0.
                                                    O.B5530
                      :    *    0.014J9
                      	O.Cl'-32__	
                               r>. •• i <^^«;      ~
                               0.
                               0.01700
                               0.01652
                               C.01993 "
                               O.C2150
                               O.C2302
                             "~~
ro
CO
 O.C30il
_0.03421_
' O.C3777
 0.04133
 O.C4439_
 0.--4338"
 O.C5193
. O.C5535_.
 O.C5876
 0-C5232
 O.C6574
"0.06915
 0.07264
 0.07593
 0.07939"
 0.05607
 p.09290_
~0.09966
 0.10634
 0- 11295_
"0.11941
 0-12544
J3. 13140_
 0". 13726
 0. 14288
 0.14854
"O. 15399"
 0. 15951
                             _
                      1.C«>20'J
                      1.13551
                      1.21'-65_
                      l .26538
                      1.^.1202
                      I. SI 1S7
                      1.60184~
                      1.67441
                      1. '373b_
                      l.Vfc5}l
                      1.96631
                      2.C4590_
                      2. U3lb
                      2- 17760
                                                    2.31C6b
                      2.
                      2.'i06S4
                      2. 43397
                      2.45341"
                                                    2.5C070_
                                                    2.51912
                                                    2.55594
                                                    .2.58336_
                                                    2.63396
                                                    2.63312
                                                    2.65615_
                                                    2.67976
                                                    2.71048
                                                    _2-73974_
                                                    2. 768 10
                                                    2.79960
AVCOX
0.99741
O.S96H
O.S9481
0.^9350
O.S9?.19
o.^goss
0.^2956
0.98824 -} ..
0.c-8692 - . •
0.'-B360
O.«8025
0.17688
0.973 49 " ~
0.97007
C.';66A3
0.'/6316
0. )5967
0. -55615
0.-/5261
0.94904
0.94544
0. 34132
C.93S17
0.934^8
0.93077 ...:.
0.92326 : :':': :: "
•'•' 0.91563 ' •'•''- .
0.90786
O.fa9997
0.89192
C. 88374 •- : ;•
c. 87539 ;;• ;:; '•.-:•. :.:
C. 86639 • . :
0.85321
0.84936
0.63107
0.81195
0.79136"
AVCOY
0.2H32S
0.39112
0.53156
O.T3975
1.55562
i • d60 ^O
2. Hb03
2.29455
2.^3669
2.59760
2.62241
2.67322
~ 2.69950
2. 7263 1
2.^533?
2.78126
2.80973
2.83848
2.b5333
2.38334
2. b98^i
2.91364
2.V2933
2.94439
2.96C60
2.99288
3.02586
3.05923
3. 09371
3.1<-671
3.20157
3.25S37 :
3.31762
3.39936
3.46347
3.64703
3.52404
4.0794<»
TRACORX
-O.d077»
-0.01 169
-0.01561
-C. 01955
-0.02351
-0.02748
-0.03147
-0. 03548
-0.03950
-0.04962
-0.05934
-0.07018
-0.03062
-0. CO 117
-0. 10183
-0. 1 L261
-0. 12350
-0. 13452
-0.14565
-0. 15692
-0. 16H31
-0.17983
-0. 1V149
-0.20328
-0.21521 :
-0.23952 .'',-
-0.26443
-0.28998
-0.31620
-C. 34312
-0.37079
-0.39924 •••'':
-0.42853
-0.45o71
-0.48982
-0.55511
-0.62496
-0.70005
ruacoRv
I.T613J
O.s
-------
                Carbon  - C - 71  -  23
  i4~  ""
= 200.  DEO F
                                                  71
                           H20
                                    U._3
                                   ""z'.O
                                    10.0
                                 SU2  =  2500.PPM
                  CG-CENTKATICN  NO  «   150.0  PPK
                           H2S04 =   72.91
                           D LOADING =   0.38 GMS H2S04/GK  C
N>
VO
Xt' GKS H2S04/GM C
0.00292
O.CC437
C.OC5SJ
O.C-Q72T
0.00375
O.C1021
0.01 167
0.01312
0.01458
O.C1S23
O.C2187
C. 02552
C. 02916
0.03231
0.03645
0.04010
0-C4375
C. 04739
O.C5104
' 0.05463
•-: ' O.C5S33 -••••-•»-."
! 0.06197 : :'. ""/-:;
0.06562 ' .,. ' .
0.06926
0.07291
C.C8020
; • 0.06749 ,
: O.C9f73 . "•••;'..' . ;,.
0.10207 :'-":, :'•.-;
0.10936
0.11666
0.12395
0.13124 :
0.13353 • 'I
0.145S2
C. 16040
0.17498
P.ATE, GMS M2S04/GK C-MIN
0.00456
0.00329
C. 00156
O.OC129
0.00113
0.00103
0.00096
0.00092
0.00039 .-./.,;;..'
- . 0.00034 >';•-
; - O.OOC33. •••'•' •••-:'^:
0.00031
0.00030
O.OO079
-. '... '.' O.OC078
. -:/.:: >,.'-:4.,' .0.00078
. :. "i ,-0.00077
0.00076
0.00076
_ 0.00075 	
~T~- -; 0.00074 ;> .:<-.:'•*
•-•'..'. •:-.:. 0.00074 S.xi*'.§
''.;'". 0.00073 "•'•":;'•»
0.00073
0.00072
0.00071
-- ' • •• , 0.00070
:. .-.;:.-;,;. •'•'•:•'• ..0.00069
'..:,.:': : '•:... ••-• ..0.00068 	
0.00067
0.00066
0.00065
-v .- . ;. ••,..." O.C0064 •:-;.:>
:;;::'.-'; '•'": ....,,, o.ooo&2 	 :^''l
'">''' '•'•" " ' 0.00061'" "•'"'^;
0.00058
0. 00055
                                                                               -S. 3^201
                                                                               -6-6'U J4
                                                                               -6.760'.<
                                                                               -o.rtSSuli
                                                                               -6. 'VI 14'->
                                                                                7.04J9&
                                                                                V.U4 ?!(>
                                                                                7.U:>046
                                                                -'-,.75744
-6.
-6.
-6.

-0.
-6.
                                                               -6.924L3
                                                               -6.91134

                                                               -b.o»204
-6 . P':

-6.K24J5

-f .77i47

-6.7^505


-6. 50367

-6.51424
-b.'
-$.'
                                                                                        0.45/f>'1
0.35<> iO
0. 33/31
0. 13002
0.32P&5
0.32124
0. 31&<>7
0 v 3 1 39 5
i! . 3 1 1 0 3
0. 30.-. 12
C. 3C'>20
0.30. -12;)
0. 3CfoO
0.2V /C.S
0.29496
0.29351
0. 29069
0.26913
0.284/6
                                                                                        0.27 JC6
                                                                                        0. 26c'6 *
                                                                                        0.26-.-U
                                                                                        0 . 2 5 •' J 4 5
                                                                                        0.254 Jb
                                                                                                                       0.24 487
                                                                                                                       •....23/17
                                                                                                                       C.22. •>!

-------
RUN riUKbER » I'D 4
_.XP^iv = , CP.S H2SC4/GM C
C-COSOi
o.-vj^s*
	 . 0.0080 5
O.CU900
O.C1015
	 . _0.011 10
~c.ci2c-4
G. j!2T-<
O.C133?
0.01',75
O.C155C
0,01333 	
o . o 2 o o <3
0.^2176
	 0.02336
0.0*74.5
0 . 0 3 1 * <•
	 0 . ."> 3 5 3 4
'0.0391'.""
O.C4293
C.f)<-&73
0.05045
C. 05410
	 0.05732 	
0.06155
0-C&513
0.06370
O.C7243
0.07615
C.C7965
0.03316
0.09024
0-0?7i3
0.10397
C. 11061
C. 11719
C. 12347
0.12952
0.13536
0.14106
0.14683
0.15259
0.l5Ei4
0.16457 •;
0.170^9
0.17355
23 71
JOST
0.«9A22
0.75277
0. 033^5
l.iO'.3'f
1.2316'.
1-3^)173 |
I.'i5?92
i.-ji-?3<.
1. 62 165
I.f.^)'i95
1.«1823
1.00943
l.-*420V
2.U6S36
2. Ii038
2.27632"
2.3cS3JS
2.^759a
2.55505
2.62058
2.675.05
2.72527
2.77263
2.81021
2. 24319
2.8^834
2.91103
2.9J392
2.95452
2.7H164
3.00521 .,-
3.C«-741
3.08700
3.12591
3.16422
3.19998
3.23976
3.28123 :
3.32435
3.36739
3.40539
3.44052
3.47739 ;:
3. 49390 ,:';
3.51936 ."
3.54369
AVCtlX
O.V'<744
0 . '; •) & 1 S
o.'y;4tih
0.<; ;JS6
0.9"2^7
0.900 I*
ti.'H.'lk;
0.'/h!>3>
0.'J'J70'.
0.9^37-j
O.9bO'. J
0.977()-»
0.9737 .i
O.O/Oii
0.-i»-694
| O.TfrSbl
0. V6000
0.95657
0.9'.i30'S
0. 94953
C.0'.5')7
0.942J8
0.93077
0.9*512
0.031',^
0.924C2
0.91647
0.90S79
0.900-JS
O.S9JOJ
'J.CU494
O.h/670
0.fa662-J
0.35973
0.85099
\ 0,63294
I O.bl40s



  •WC'.IY
I'.S* ?:>•>
o. r i*Q-i i

i.•/ }'•'<•>
2 . 5'/ < '11
;'. /<•.-: 2 7
3. I'1521
3.21500

3.27653
3, JJ314
3. J245J
3.35705

3. 41) 70 d
3.4', 127
i , 4 < 0 o 3

3.5/1557
3.o234u
3.
3.n6'J2'J
3 . -! i 5 6 2
4.D2329
«... 10056
4. 30710
4.5349S
                   - 0.0 ' 11 H
-r,..',6:)5i
-o.o.'-;>'5


-0.11152
-0.12230


-O.IU5J7
-0.16664
-0. 1/504-
-0.18957
-0.2012*
-0.21 3,!3
-C.23706
-0.26692
-0.31252

-U.31671

-C.4X367
-0.45342
-0.4j;40d
-0.54837
-0.6170o
                       ;).'..il /••

                      -o.'.7-, n
                      -U . 6'»'/ a1,
                      -, 1 , / •) / -J ^
                      —' I . •". )-i f L-
                      -0. -•> U 7

                      -I .'J31 )•)


                      -1.1
                                            .l'.(2 7
                                            . 1 >f v?
                                            . I 'j 7 d -i
                                            .17727
                                           i. n;&7o
                                           i. nc-jy
                                          -1./-U'
                                           1.2'V'Jb7
                                           1.21612
                                           1 .
                                           1.2 >H05
                                           1.31420
                                           1. 33062-
                                           1.3->30:>
                                           1.37S12
                                           1. 3^334
                                           1.41 112
                                           1.4-^027
                                           1.51182

-------
Car-bra  C - 71 - 23
                               71
TEv.PERATURc » 200. OEG F
TOTAL FLOW  RATE = icoo.o CC/MI.N
         cri2  =_
        ~ '02'*=
Pb^CENT  M2C  =
_
  2.0
 10.0
CG^CfcMTRATIO'l S02 = 1500.0  PPM
CONCENTRATION  NO =  130.0  PPM
3fcRCc'.T  H2S04 =  74.
SAIuKATED  LOAOING =
                     01
       0.3B GHS H2S04/GM  C
X, GKS H2SIA/GM C
0.001«3
0.00296
0.00444
0.00592
O.C0740
O.OCS83
0.01036
0.01184
O.C1332
0. 01*60
0.01850
0.02220 .
0.02590
0.02960
0.03330
0.03700
O.G4071
0.04441
0.04811
O.C5181
: , 0.05551 ;:.
0.0592!
0.06291
0.06661
0.07031
0.07401
0.03141
0.08881
0.09621
0.10361
0. 11101
0. 11842
0.12582
: 0.13322
0.14062
0. 14802
0.16282
0. 17762
0.19243
P.ftTS, GKS H2S04/GM C-H1N
0.00512
0.00422
0.00232 .. : •: . •....
C. 00114 . ... I/....:.
o. 00094 . > .';••:. ';••'-
C.OOOS4
O.OC073
0.00075
0.00074
0.00073
0.00072
0.00071
0.00070
0.00070
0.00063
- . '..' 0.00068
. 0.00067
O.C0066
0-00066
0.00065
.:: . - • 6.00064
••'•'•'. . . 0.00064.
0.00063
C.OC063
0.00062
0.00061
• ; . . . . C.OC060
0.00059
*1'-', ^: . O.C0058
0.00057
0.00055
0.00053
0.00052 ; :'.: .-' :'
• :.:'V.;--- ?JUVC" • 0.00050 •-::^-^:^i
"•". " 0.00043..' "?;::••".
0-OOC46
0.00042
0.00039
	 " -' 0.00034
                                                                     weSTVACO
                                                                     -5.27107
                                                                     -5.46018
                                                                     -6.C5457~
                                                                     -6.75975
                                                                     -6.95501
                                                                     -7.C6339"
                                                                     -7.12310
                                                                     -7.16223
                                                                     -"7.17805"
                                                                     -7.18020
                                                                     -7. ia4Q2_
                                                                    ""-?. Id913
                                                                     -7.18921
                                                                     -7. 10917_
                                                                    "->. 1945J
                                                                     -7.19466
                                                                     _-7.19469__
                                                                     -7.19483
                                                                     -7.19486
                                                                     -7.19300
                                                                     -7.18939"
                                                                     -7.18357
                                                                     r7.'lS358
                                                                    '-7.18348"
                                                                     -7.17753
                                                                     r7. 17747_
                                                                     -7. 17'l"09
                                                                     -7. 16442
                                                                     -7.15745_
                                                                     -7. 15667
                                                                     -7.15584
                                                                     r.7..16.187_
                                                                     -7.16114
                                                                     -7.16774
                                                                     -7.17478
                                                                     -7.18217"
                                                                     -7.20771
  MODWESTVACO
     -5.26717
 	-5_.452J5_
     -6.0~423~1
     -6.74404
    _-6.93535
     -7.03974'
     -7.C9545
 	-7.13062
     -7.~i42.V7"
     -7.1-4947
 	 -7.13411
    "-7. 12893"
     -7.11861
 	-7.1CS07

     -7.CV221
 __	-7.03139
     -'7.07056 '
     -7.C5950
 	^7.04843
     -7V63143""
     -7.01419
     -6.99076
     -6.97293
_^	-6.96085
    "-V.92998"
     -6.89322
     -6.86550
     -6."83»2"9~
     -6.61032
     -6.7 B 84 5_
     -6.75903
     -6.73607

     -6.6S365
     -6.64326
     -6.59796
                                                                                                  AMUNUSON
                                                                                                 " 3.41206
                                                                                                  2.U1312
                                                                                                  I. 54646
                                                                                                 ~b.7o097
                                                                                                  0.62351
                                                                                                  0.55725
                                                                                                  0.52286
                                                                                                  0.50075
                                                                                                  0.49093
                                                                                                  0.48J53
                                                                                                 0.47376
                                                                                                 0.46B8J
                                                                                                 0.46394
                                                                                                 0.45659
                                                                                                ~
                                                                                                 0.44677
                                                                                                 0.44184
                                                                                                 0.43696
                                                                                                 0.43202
                                                                                                  _
                                                                                                0.42714
                                                                                                0.42220
                                                                                                0.40992
                                                                                                0 .4025 7 _
                                                                                                0.39V2I
                                                                                                0. 38786
                                                                                                P-.3J804 __
                                                                                                C.3~6t>22
                                                                                                0.35594
                                                                                                Q. 3.1 6 1.2 _
                                                                                                0.33383
                                                                                                0.32155
                                                                                               .P.. 30931 __
                                                                                                0.28227
                                                                                                0.25775

-------
                 RIP! NU
                                141
                                          4 26 71
                       0.00449
                       0.00619
                       U. 00722
                       O.OObOj"
                       O.CCS34
                       C.CC956
                       O.C1G2*
                       0.01093
                       O.C1171
   JOST_
6.33390
0. 45487
0.62362
C.'7471V"
CO
                        0.01 392
                        0.0153^
                        O.C16S7
 0.02342
 0.02703
 C.03063
 0.03402
 0.03726
 0.04J51_
"d.04367
 0.04676
 0.04993
 '0.05392
 0.05597
 0.05699__
"0.06201
  .06510
  .0/.312
  .07114
  .07703
  .Cc<285_
  .03S59
  ,09426
  .09979
  .10560
  .11120
  .11643.
 C" .'12188
 C.12710
 0.13219
""O.:13719
 0.14223
_0.14728_
 6715207
 0.15663
 C-16I05
"0.16532"
 0.16945
 i'Vu 2 533
 1.09333
 1 .15302
 l'. 2 04 9 7
 I.RT29S
 1.3f>4'6
       "
                                             1.47222
                        0.
                        C.
                        0.
                        0.
                        O.
                        0.
                        0.
                        0.
                        0.
                        0.
                        0.
                         "
 I .60142
 1 .66491
 1.71385
 1.76354"
 1.61140
_1 . 65 1.5V
 1~.V:J9"34
 1.92A74
 1.95285
 l.Vb036
 2. C 1C 14
 2.03_433_
 2.05626
 2.07376
 2.09193
 2.L3B57
 2. 14203
 2. 17269
 2.20115
 2.22790
 2.25479
 2.27262
 2-29316
                                             2.33337
                                             2.36026
                                             2.38295
                                             "2.40538
                                             2.42465
                                             2^444 3 3
                                             2.46600
                                             2.48987
                                             2-51i70
                                                  "
AVCOX
0.99870
0.99740
0.9V609
0.9947!',
>,. 0.99347
0.99Z15
0.-90083
0.90950
• 0.98B1 r .
0.98684
0.93350
0.98013
0.97674
0.97333
0.96989
0.96642
0.96294
0.95942
0.9558B
0.95232
0.94873
0.94510
0.94146
0.93773
0.93407
•• 0.93034 : ; ' .
0.9227H :: :
0.91509
0.90727
0.89931
0.8912;. . '
0.88296 . ;.:i, -
.0.87456 ,~ ;;:::,; :..
0.86598
0.85724
0.84831
0.82987 .-.'-, :•,
o.8io57 •'• ::
. -.0. 7903). : ':O:-
4VCOY
0.2930B
0.35548
0.64&64
1-31411
1.60382
1. 794 54
. 1.91257
1.99700
2.03694
2.06011
2.07851
2.11076
2.13297
2.15543
2.19014
2.21406
2.238Z7
2.26326
2.^dS56
2.31470
2.32799.
2.34117
2.36853
2.39625
2.41051
2.43952
2.4«<-07
2.5302S
2.57824
2.64520
2.71573
2.B0947
2.8S917
2.99550
3.10995
3.23298
3.54266
• 3- £7? 70
4.3SC27 :
                                             2.5670!>
                        cYi7696
                        0.18057
                        0.16389
                        0. 16742
  2.62774
  2.65325
  2.691 90_
  2V72122
  2.75043
  2.731II_
TR4CORX
-0.00390
-0.00732
-0.01175
-0.01570
-0.01967
-0.02365
-0.02765
-0.03166
-0.03069
-0.03973
-0.04992
-0.06021
-0.07060
-0.08111
-O.C9172
-0. 10246
-0. 11330
-0.12427
-0-13536
-0. 14657
-0.15791
-0. 16938
-0. 18098
-0. 19272
-0.20460
-0.21662 :
-0.24110
-0.26620
-0.29195
	 -0.31837 	
-0.34552
-0.37342 . ::.y'::
1 	 ^0.40212 	 ..;..,..,.
-0.43167
-0.46211
-0.49352
-6.55945. ' ::.;v
-0.63004 .;.;-.. :- .,.
( -0.70600 : .

TSACURY
l.iT273l
1.03429
0.'-3597
-0.27316
-0.47239
-U. 58475
-0.648<-5
-0.69165
-0.71 145
-0.72664
-0.73165
-0.74705
-0.75752
-0.76799
-0.7S i96
-0.79483
-0.30570
-O.S1681
-O.B27V3
-O.i',3928
-0.64501
-O.t5065
-0.66227
-0.67391
-O.U7934
-O.b9lo0
-0.90990
-0.92333
-0.94711
-0.97275
-0.99906
-1.03300
-1.06097
-1.C57U
-1.1346:.
-1.17343
-1.26488
-1.35576
-1-47711

                         0. 19596

-------
                Carbon- C - 71 -  23
                     NUM9E'R'«~  142  	4 27~7l	
                 TEr-PERATUKE =  200.  OtG F

                 TOTAL  FUGw RATC"~= "i~aQ0.6~ CC/MTN
               ..PfcB,CENr_CLi2 =	11.3_
                Pt^CENr   02 '-'  "2/0
                PLD,CEMT  H2U =   10.0

                CC\c E'l r p.Tr i ON" sof" *~ iTJoo". O~"PPM"
                CCNCENTRATION  NC =   150.0 PPM
                PERCENT  H2S04 =""71.88"               	"
                       TED LOADING =    0.38 (JHS H2S04/GM  C
U>
u>
X, G."!S H2SC4/GM C RATE,
0.00144
0.00238
0.00431
C.OC575
0-U'J719
O.CQ863
0.01006
	 0.01150
0 . U 1 2 9 '•
0.01433
	 0 . 0 1 7 J 7
C. 02156
0.02516
O.C2375
0.03235
0.035V4
0.03953
0.04313
0.04672
' 0.05032
0.05391 r- """' ' "
0.05750
O.C6110
C.D6469
0.06S29
O.C7133
0.07907
0.06626
0.09344
0.10063
0. 10782
0.11501
0.12220
0.12933
0.13657
0.14376
0.15814
0.17251
&>.S H2SC4/GI'. C-MIN
0.005C4
C. 00363
0-00214
O.OOC96 '" ' ri.'.V.
O.OOCB3 -::':""~
0.00076
0.00071
0.00067
0.00066 •. .: •;
C. 0006 5 •' •-'•: -:>'<,•
O.OC064 -,;:. .,;.".
0.00063
0.0.0062
C. 00052
O.OOC61
0.00060
0.00059
0.00059
0.00058
0.00058
0.00057 .. .. ..':,; '-:'•-.
O.OQC56 ''"f;,':-;5vy::::;
0.00056 -:-:i-:-::'-.
0.00055
0.00054
0.00054
0.00353 r : "
.: 0.00052 .-;.S;::M
0.00051 -': •'/;• " '
0.00050
0.00049
0.00047
0.00046 ,••:.: •••- w -
0.00045 :: ^:>:r -:;;
O.Cf,043 '"• •""•"•"•'
O.COC42
0.00039
0.00035
H6STVACO
-5.28716
-5.59679
-6. 13647
-6.92926
-7.070R4
-7.16276"
•••••-• -7.22813
-7.27152
-7.29485
-7.29653
-7.303'.'.
.. ' -7.30484
-7.31203
-7.31357
-7.31514
-7.31662
-7.31826
-7.3199V
-7.32166
••"... -7.31704
-.7.31876
-7.32052
-7.31573
-7.31749
.'•'•. -7.31929
.•;:; '.:"• -7.31433
-7.31117
-7.30772
-7.30411
-7.30034
',;•- -7.29652
-7.29237
-7.28SOO
-7.29152
-7.29510
-7.2V909
-7.30771
	 __ -7.317.81,
MOO«ESTVACO~"
-5.23337
-5.50919
-fa. 12506
-6.91402
-7.C5175
-7.13930
-7.20129
-7.24079
-7.2t
-------
                          RU\ r.UKS
                                         142
                                                    4 27 VI
OJ
XPRIME, nvS H2SQ4/GM C
0.004^.9
0.00551
0. 00652
0.00 O2
o. tea 19
0.00',J06
C. 00973
0.01051
0.01123
C. 01189
0.01312
0.01^35
0.01566
C.C1696
O.Ciy26
0.0213o
0.02450
0.02754
0.03073
0.03377
0.03667
0.03957
C.C4247
0.0'.537
0.04320
C. 05109
0.05370
0.05531
C. 05906
0.06167
O.C6435
O.C6950
0.07501
0.08059
O.OS61C
O.C9146
0.096? 7
0.10211
0.10726
0.11243
0. 1174S
0. 12241
0.12719
0.13161
0. 13633
0.14089
0.14531
0. 14959
' 	 0.15394 ~ . , ." -
0.15814
0.16205
0.16575
0.16640
JCST
0.22259
0.36324
0.4',016
0.54664
o . fc ; o 7 1
O.S6243
0.71554
C -7A126
O.t'JlOo
0.84112
0-91477
O.°7560
1.02201
1.0^154
1.C-J501
1. Ift9^7
1.22465
1-27101
1.. 301 71
1.33257 ;
1.36339
1.36994
1.412S7
1.4326^
1.'.5242
1.46793 ,::/-':
1.4S971 -•".
1.50948
1.52373
1.54036
1.57390 •;;••
1.58272 . .
1-59970
1.61307
1.62606
i. 64006
1.65251 .•:
1.66483
1.67813 ._
1.66922
1.70241
1.71552
1.72967 --..•••.••
i.74756 :.:,;••:':
1.76C46 ....
1.77441
1.76925
1.60494
1.81891 ,. ,,.
1.S3366 '-i
1.E5124
1.S7031
1.37497
| /VCOX
I6.TVU74
0.^9747
, 0.r.V620
j 0.<:9',93
0. '.9.165
0 . T 9 2 3 S
0.99109
o.?8?si ; .-.; ;
0-?bH52 -'':'
0.98723
0.98398
0.98071
0.97743
0. 97M1
0.^7073 • •.-.
0.96742
0. '76 404
0.96064
O.S5721 .. ' . ..
C. 953 76 ..: '• : • •'•
j 0.95023 : . -
|! 0.9-'i678
?S C. 94325
0.93969
0.93610
0.93249
0.92518
0.91776
0.91021
0.93254
O.B9473 , :..
. 0.83678 : ., ..;.:.• ;
0.67S69 .-•• ';"";- •--.' '':.
0.67045
0.85204
0.85347
0.8*580
,0.81734
;'" .
AVCUY |
0.1 ,'853 |
0.27161 !
0.4c>773
l.'037ii
1.H963
1.32043
1.41512
1.48364
1.324&1
1.5331S j
1.S5912
1.57697
I.tj-4i4
1.62335 !
1. 6^-270
1.66233
1.68264
1.71345
1.7247d
1.75554
1 . 757S8
1.7B040
1. 7V 187
1.S1549 \
l.y'3973 ' 1
I.SS198 j
l.«"023 , [
1.92982 |
1-97111 I
2.01^20 S
2.Ci?5i ||
2.10661 . I
2.15591 1
2.22558
2.29951
2.37895
2.55502
Z.75979 ^; |
TRACORX
"-O.CC37-7
-0.00760
-0.01141
-0.01523
-C.OIOIO
-0.02296
-C.026S4
-O.U307J
-O.U3464
-U,C3b5?
-0.0^^44
-0.03342
-0.06850
-0.07868 --
-O.CR096
-0.0-3936
-0. 10986
-0. 12047
-C. 1311'/"
-0. 14204
-0.15300
-0. 164C3
-0. 17529
-0. 18662
-0. 1930S
-0.20968 ••. .'..
-0.23329
-0.25746
-0.23224
-0.30764
-0.33371
-0.36047 . -•:.....: -.,.
-0.38797
-0.41625
-0.44535
-0.47532
-0.53811
-0.60510
TRAC01Y
1 . H 6 8 1
1. Vj337
0. T59J7
-IJ.U36/6
-O.I. "..'18
-0.27/96
-0. .14722
-0.3)450
-0.42174
-C.'.2M4
.. -0.44412
-0.45551
-O.'f /2f f
-0.4644^
-O.f<634
-C.&0322
-0.52036
-0.53266
-0.54510"
-0.55132
-0.56400
-0.576S4
-0.56326
-0.59635
-0.60962
-0.61626
-0.63670
-0.65743
-0.67860
-0.70022
-0.72247
-0.74508
-0.76821
-0.30002
-0.83270
-0.86666
-0.93SC6
-1.01515


-------
                   Carbon- C - 71 -  23
                     1U?1 M!ft»ea=   143'      4 28 71
                     TE.-'PErt.-.TURE =  200.  DEG F
                           FLCU RATE =  1000.0 CC/MIN
 Pf'.CENT C02  =
"ptHCENT  C2  =
 PfcRCENT H20  =
                                      11.3
                                       2.6"
                                      10.0
                    CC-;CE\T3AUON S02
                    CUNCE.'JT«AT;ON  NO
                       500.0 PPK
                       150.0 P?;I
                     PERCENT H2STV »   72.45
                     SATURATED LOAOlMG  =    0.33 GN'S H2S04/GM  C
Ul
X, r.l'S ii2StJ4/GK C RATE,
0.00145
O.C0290
O.OOA35
O.C0530
0.0072^
0.00869
O.C10U
O.OH;.'?
O.C130'.
O.C1A49
O.CiSil
0.02173
C. 02536
0.02893
C. 03269
0.03623
0.03935 : .. • .
0.043
-------
CO
                                     O.CJ32',
                                     O.C-/4'./
                                     'J. 0'. ii'j
                                      0 . C 0 'i '! 7
                                      O.C1195
                                      O.C13^'<-
                                      O.C14C6
                                      0 . 0 i 5 'J 'J
                                      0.01 739
                                      0.01963
                                      0.02195
                                      C. 02^-2 6
                                      0.02651
0.0307D
O.OJ26"
0.03506
C.C.-370J
0.03912
0.04iCO
0.04317
O.C4527
0.04 73d
0.04933
C. 05 324
0.05715
0.06099
0. 064o3
0.0686D
0.07251
0.07664
0.06055
O.CE'53
  CB
                                     a. | ...-,•,.
                                     'j . i f> 3 7 1>
                                                           0.3 :
                                                           0.4>3/o
                     0.<-'-U49
                     0.50745
                     0.55210
                     0.54557
                     O.ol345
                     0.04033
                     0.66679
                     0.7L3B9'
                     U.7o426
                     0.79744
O.S/160
O.AV312
  912'27
  V2702
  94372
  95H69
  v/562
  96441
  99395
1.00264
1.01356
1.03299
1. 04990
1.C6578 "
1.07977
1. 09-336
1.10333
1. 10912
  11732
  12380
  13062
  137o5
  14614
  15130
  15850
  16442
  L6918
1.17362
1.1784'J
l.ld'3/6
1.1 5140
1.20286
1.21169
1.22141
1.23070
1.23895
1 .24999
HUN NUMOtR =






































AVCUX
0 . fi 9 <3 7 3
0.99745
0.99617
0..99489
0.99360
0.99231
0.99102
0.9d97 1
0.9ciB4.i
0.98712
0.983B5
0.98056
0.97724
0.97390
0. V 7O54
0.16716
0.96375
0.96031
0.95686
0.95337
0.94986.
0.94633
0.94277
0.93918
0.93556
O. 93192
0.92454
0.91705
0.90943
0.9016b
0.89379
0.8S576
..O.H7759
0.66926
C.S6076
O.S5210
O.fc3422
1*3 4 28 71
A'/CCY
0. 1<.{J44
C . 2 j 1 6 5
0.4/605
0.00022
0.71531
0 . (-. I 2 I 1
0. '•••)& 5 1
0. J'.>ti^5
1 . '••) 764
1.03795
1.05380
1 . U / h-j 0
1.0J562
I. 13439
1.12235
1.14090
1-. 15041
l.lf.008
1. 1 /991
1. 1-^009
1.20044
1.2109/
1.22169
1.23260
1.24370
I.2o501
	 	 1.26653
1.29021
1.31479
1.34032
1. 36637
1.31449
. 	 _ 1.43307
1.46866
1.50061
1.55120
1.6633/
TRACCRX
-0.003112
-O.OC7t>6
-O.U1151
-0.01537
-0.01925
-0.02314
-O.C2705
-0.03098
-C.03'»l>2
-0.03C33
-0.0223
0-r>1046
0.33504
0.20012
0. 10925
0. 04223
-O.OJ761
-O.U3724
-0.05240
'' -0.07557
-0.0)132
-0.09929
-0.11542
-0.13102
-0. 14012
__ -0.14849
-O.i6544~
-0. 1740J
-0. 18269
-0. IV 142
-0.2002J
-0.20912
-0.21809
-0.22714
-0.23626
-0.2:>480
-0.27367
-0.29291
-0.31252
-0.33253
-0.3633O
-O.i8436
-0.40587
	 -0.43903 	
-0. 50884 ~
                      1.25VU5
                      1.26564
I ..
1.
                        • / 710
                         .". 5 9 O

-------
    CARBON C - 71 -23
r
c
c
f
    RUM NUnJEK  =   144 - 6    4 29 71
    TEMPERATURE =  200.  DFT, F

    TOTAL FLOW  RATE  =  1000.0 CC/MIN
PERCENT  C02 =   11.3
PERCENT   02 =    3.5
PERCENT  H20 =   10.0

CINCFMTRATIOU SU2 =
CONCENTRATION  NO =
2000.0 PPt-i
 150.0 PPM
PERCENT  II2S04  =   73.31
SATURATED LOADING =   0.38
       CMS H2S04/GM C
    X,  CMS  H2SD4/GM
           0.00293
           0.00440
           0.00586
           0.00733
           0.00880
           0.01026
           0.01173
           0.01320
           0.01466
           0.01833
           0.02199
           0.02566
           0.02932
           0.03299
           0.03665
           0.04032
           0.04399
           0.04765
           0.05132
           0.05498
           0.05865
           0.06231
           0.06598
           0.06964
           0.07331
           0. OP,064
           O.CH797
           0.09530
           0. 10263
           0. 10906.
           0.11730
           0. 12465
           0.13196
           0.13929
           0.14662
           0.16120
           0.17594
           0.19061
           0.20527
                        RATtt GPS
              H2SD4/GM C-MIM
                 0.00')3'j
                 0.00375
                 0.00253
                 0.00155
                 0.00143
                 0.00136
                 0.00 130
                 0.00125
                 0.00120
                 0.00114
                 0.001)0
                 0.00108
                 0.00107
                 0.00106
                 0.00105
                 0.00105
                 0.00104
                 0.00103
                 0.00103
                 0.00102
                 0.00102
                 0.00101
                 0.00101
                 0.00100
                 0.00100
                 0.00009
                 0.00098
                 0.00098
                 0.000-J7
                 C.00095
                 0.00094
                 0.00092
                 0.001)90
                 O.OOOH3
                 0.00085
                 o.oooai
                 0.00076
                 0.00071
                 0.00065
                                                           WESTVACO
                                                           -5.22311
                                                           -5.57390
                                                           -5.96561
                                                           -6.45310
                                                           -6.529)8
                                                           -6.5/599
                                                           -6.61390
                                                           -6.64786
                                                           -6.68315
                                                           -6.73022
                                                           -6.75328
                                                           -6.76000
                                                           -6.75996
                                                           -6.75647
                                                           -6,75285
                                                           -6.74930
                                                           -6.74547
                                                           -6.74165
                                                           -6.73775
                                                           -6.73019
                                                           -6.72252
                                                          -6.71465
                                                          -6.71045
                                                          -6.70235
                                                          -6.69421
                                                          -6.67745
                                                          -6.66023
                                                          -6.64235
                                                          -6.62774
                                                            .61648
                                                            .60074
                                                            ,59237
                                                            .58774
                                                            ,58284
                                                          -6.57766
                                                          -6.57099
                                                          -6.56341
                                                          -6.55990
                                                          -6.55583
-6.
-6.
-6.
-6.
-6.
                                       37

-------
     CAKfiON C - 71 - 23
     RUN NUMBER =   145  - G    A  30  71
     TEMPERATURE =  200.  DEC  F.

     TOTAL FLOW RATE  =  1000.0 CC/MIN

     PERCENT  C02 =    0.0             	
     PERCENT   U2 =    2.0
     PERCENT  H20 =    10.0

     CONCENTRATION  S02  =  2000.0 PPM
     CONCENTRATION   NO  *   150.0 PPM

     PERCENT  H2S04  =  72.61
     SATURATED LOADING  =   0.38 CMS H2S04/GM  C
r
X, CMS H2S04/GM C
       0.00290
       0.00436
       0.00581
       0.00726
       0.00871
       0.01017
       0.01162
       0.01307
       0.01452
       0.01815
       0.02178
       0.02541
       O.Q2-904
      - 0.03267
       Q.03630
       0.03994
       0.04357
       0.04720
       0..05083
       0.05446
       0.05809
       0.06172
       0.06535
       0.06898
       0.07261
       0.07987
       0.08715
       0.09439
       0.10165
       0.10891
       0.11618
       0.12344
       0.13070
       0.13796
       0.14522
       0.15974
       0.17426
 RATE, CMS H2S04/GM C-MIN
             0.00648
             0.00-315
             0.00378
             0.00266
             0.00148
             0.00107
             0.00102
             0.00099
             0.00097
             0.00093
             0.00090
             0.00088
             O.OOOB6
             0.00085
             0.00083
             0.00082
 	...0.00081 _	
             0.00080
             0.00079
             0.00078   	
             0.00078
             O.Q0077
            .. 0.00076
             0.00076
             0.00075
             0.00074
             0.00073
             0.00071
....	      0.00070  ...
             0.00068
             0.00066
             0.00064
             0.00062
            ' 0.00060
         	 0.00058
             0.00054
             0.00049
WESTVACO
-5.03189
-5.25814
-5.56315
-5.90916
-6.49575
-6.81763
-6.85510
-6.87969
-6.89768
-6.92936
-6.95062
 /  O f f t f\
 O » t »_» -t O. w
-6.97495
-6.98562
-6.99227
-6.99475
-6.99720
-6.99980
-6.99788
-6.99591
-6.99390
-6.99185
-6.98985
-6.98771
-6.98069
-6.97128
-6.96638
-6.96125
-6.95599
-6.96094
-6.95527
-6.96048
-6.96029
-6.96599
-6.97220
-6.98572
-7.00892
                                       38

-------
CAHUON C - 71 -23

RUN NUI-'HCR  =   140 -=• G    5
TEMPLRAIUKE =  150. DEG  F
                                 7  71
     TOTAL FLOW RATE = 1000.0 CC/HIN
(

C
PERCENT C02 = 11.3 ........ j
PERCENT . 02 = 2.0
PERCENT H20 = 10.0
CONCENTRATION S02 = 2500.0
CONCENTRATION NO = 150.0
PERCENT H2S04 - 57.18
SATURATED LOADING = 0.38
X, GMS H2S04/GM C RAT
0.00229
0.00343
0.00457
0.00572
0.00686
0.00801
0.00915
0.01029
0.01144
0.01429
0.01715
0.02001
0.02287
0.02573
n.O?R59
0.03145
" 0.03431 . . 	
0.03717
0.04003
0.04288
0.04574
0.04860
0.05146
0.054-52
0.05718
0.06290
0.06862
0.0743 1
0.00005
0.08577
0.09149 -:
\
0.09721 	
0.10292
0. 10864
0. 11436
0. 12580
0. 11723
0.14067
0. 16010
0. 17154
0.18290 ._... .
0. 19441
0.20585
0.21728 .. ..



PPM
PPM

GMS H2S04/GM C
Et -GMS H2SU4/GX C-MIN
0.0? 170
0.02000
0.01C44
0.01705
0.01572
0.01447
0.01331
0.01??. 4
0.01122
O.OOB75
0.00671
0.00513
0.00416
0.00380
0.00351
0.00326
	 	 __;.'. 0.00303 	
0.00283
0.00269
	 	 . 0.00257 	 	
0.00248
0.00238
0.00230
0.00?23
0.002L6
0.00203
0.00191
0.001BO
0,. 00 169
0. 00160
0.00151

0.00142
0.00133
0.00125
O.fJOll?
0.00102
0.00089
0.00078
0.00068
0.00059
0.00052
0.00044
0.00037
. ....... ..;.. 0.0003 I.
                                                           WESTVACO
                                                           -3.82459
                                                           -3.90312
                                                           -3.93119
                                                           -4.05639
                                                           -4. 1 346?
                                                           -4.21415
                                                           -4.294 71
                                                           -4. 3/59?.
                                                           -4.459 04
                                                           -4.70013
                                                           -4.95756
                                                           -5.21921
                                                           -5.41930
                                                           -5.50237
                                                           -5.57331
                                                           -->,64U4H
                                                             ,70435
                                                              76372
                                                             .80662
                                                             .84341
                                                             .87305
                                                             ,90176
                                                          -5.92937
                                                          -5.95318
                                                          -5.97538
-5,
-5«
-5,
-5,
-5.
-5.
                                                                 .01697
                                                                 .06203
                                                                 ,10466
                                                                 , 14423
                                                                 .18355
                                                                 .22233
                                                                 .26035
                                                                 .30579
                                                                 ,35135
                                                                 ,39535
                                                                 .40620
                                                                 .57693
                                                                 ,66498
                                                                 .74676
                                                                 .82689
                                                              -6.91357
                                                              -7.02084
                                                              -7.12669
                                                              -7.24405
                                                          -6,
                                                          -6,
                                                          -6.
                                                          -6.
                                                          -6.
                                                          -6,
                                                          -6.
                                                          -6.
                                                          -6,
                                                          -6.
                                                          -6.
                                                          -6,
                                                          -6,
                                                          -6.
                                                          -6,
                                      39

-------
CARBON C  71 - J>3
RUN NUKKI:R  =
TLMPLKATIMC  -
149 _ G
150. DEG
    5 10 71
TOTAL  PLOW  RATE  =  1000.0 CC/MIN
PEI'CLNI  C02  =
PERCENT   02  =
       T  H20  -
CONCENTRATION
CONCENTRATION
  11.3
   2.0
  10.0

502 =
 NO =
1500.0
 150.0
                                 PPM
                                 PPM
C

C
PERCENT  H2S04  =   56.66
SATURATED  LOADING =   0.38 CMS H2S04/GM C
    CMS
H2S04/GM
0.00569
  C0682
  00796
  00910
  0102 5
  0113/
  0142 I
  01706
  01990
  02274
  02559
  02843
0.03127
0.03412
  0 -)ty:jo
  03980
  04264
  04549
  04833
  05117
  05402
  05686
  06255 ..
  06023
  07392
  07960
  09529
  09098
  09666
  10235
  10 « 0 J
  11372
  12509
  13646
  14784
  15921
  17058
  1819S
  19332
          RATE,
        0,
        0.
        0.
        0.
        0.
        0,
        0,
        0,
        0.
        0.
        0.
CMS H2S04/GM C-MIN
       0. 0 l'i 1 I
       0.013/1
       0.01241
        .01122
        .01020
        .00925
        .00712
        .00548
        .00424
        ,00348
        .00291
        ,00259
        ,00220
        ,00202
        .00190
        .00182
        ,001.76
        ,00171
        ,00168
        .00164 	_
        .00161
        ,00158
        ,00152
        ,00146
        .00140
        .00135
        ,00131
        .00125
        ,00120
        .00114
        ,00109
        ,00103
        ,00091
        ,pO()79
        .00068
        .00058
        ,00049
        ,00040
                       0.
                       0.
                       0,
                       0.
                       0.
                       0.
                       0,
                       0.
                       0,
                       0.
                       P-
                       C.
                       0.
                       p.
                       0.
                       0.
                       .0.
                       0.
                       0.
                       0.
                       0.
                       C).
                       0.
                       0.
                       0.
                       0.
                       0,
                       0.
                       0.
                       0.
                       0.
                       0.
                       C.
                       0.
                       0.
                       C.
                                       WKSTVACO
                                       -4.17746
                                       -4.27187
                                       -4.36807
                                       -4.4655r>
                                       -4. 1^827
                                       -4.6'i23f)
                                       -4.90639
                                       -5.16134
                                       -5.41044
                                       -5.59894
                                       -5.76863
                                       -5.87837
                                       -6.03522
                                           10890
                                           16141
                                           19770
                                          22552
                                          24193
                                          25409
                                          26661
                                          2/781
                                          28935
                                          31173
                                          33356
                                          35289
                                                            -6.
                                                            -6.
                                                            -6,
                                                            ~~O i
                                                            -6.
                                                            -6,
                                                            -6.
                                                            -6.
                                                            -6.
                                                            -6.
                                                            -6.
                                                            -6.
                                                            -6.3713.8
                                                            -6.
                                                            -6,
                                                            -6,
                                                            -6,
                                                            -6,
                                                            -6,
                                                            -6.
                                        00033
       0.20470
                       0.00028
                                         .30677
                                         .40949
                                         .43368
                                         .45950
                                         .48964
                                         .52466
                                         .60669
                                       -6.70137
                                       -6.80490
                                       -6.91410
                                       -7.03421
                                       -7.16077
                                       -7.29206
                                       -7.41469
                                  40

-------
c
c
c
c
c
c
c.
    CARBON C  - 71  - 23

    RUN  NUMBER  =   150 - G    5 11 71
    TEMPERATURE =  150.  DEC F
    TOTAL PLOW  RATE  = 1000.0 CC/MIM
PERCENT CU2 =   11.3
PERCENT  02 =    2.0
PERCENT H20 =   10.0
CONCENTRATION S02 =  500.0 PPM
COMCEiURAI ION  NO =  15C.O PPM
PERCENT II2S04 =  53.33
SATURATED LOADING =   0.38 CMS  H2S04/GM  C
   CMS
H2S04/GM C
0.00427
0.00534
0.00640
0.00747
0.00051
0.00960
0.01067
0.01333
0.01600
0.01867
0.02133
0.02400
0.02666
0.02933
n, n.\?oo
0.03466
0.03733
0.04000
0.04266
0.04533
0.04800
0.05066
0.05333
0.05866
O.OC.400
0.06933
0.07466
0.07999
0.00533
0.09066
0.09599 ..v
0.10133
0.10666
0.11733
0. 12799
0. 13866
0.14932
0. 1 5999
0. 17066
0. Hi 132
RATE, CMS H2SG4/GM C-MIN
0.01620
0.01322
0.01123
0.00956
0.00815
0.00694
0.00591
0.00394
0.00268
0.00187
0.00146
0.00121
0.00112
0.00104
0.001.0]
0.00100
0.00098
0.00098
0.00097
0.00096
0.00095
0.00094
0.00093
0.00091
0.00090
O.OOOH7
0.00085
0.00083
0.00081
0.00078
0.00076
0.00074
0.00072
0.00067
0.0*0062
0.00056
0.00049
0.00042
0.00034
0.00026
WE3TVACO
-4. Ill 34
-4.31159
-4.47216
-4.62934
-4. 78685
-4. 94486
-5. 10.142
-5.50164
-5.&UO/6
-6.23278
-6.46898
-6.65079
-6.72350
-6.78601
-6.60707
-6.81275
-6.82027
-6.81757
-6.82009
-6.82261
-6.82518
-6.82513
-6.62776
-6.83325
-6.83043
-6.64194
-6. 85099
-6.81)736
-6.86407
-6.87 744
-6.88821
-6.89606
-6.91 140
-6. 94459
-6.98196
-7.04219
-7. 11253
-7.23136
-7.3B840
-7.59702
                                       41

-------
     CARBOii C - 71 - 23

     RU', raJ,'mi:R  =   131-G    51271
     UM'r'LKAIURE  = 300. DEC F
C
c;
c
r
TOTAL I:LUU  RATE  - 1000.0 CC/MIN

IMiKCEiJT Cu2  =    1.1.3
1'hRU.NT   02  =     2.0
I'tf'.CLIil H2C  =    10.0
Ct/MLtKTRM I(J-\I  Su2 -
GU.-iCEuTRATlUN   NO =
                     2 '300.0 I'PI"
                      150.0 PPM
      T II2SU4  =   81.86
SATURATED  LOAIJI.MG =   0.38 CMS H2S04/GN C
        CMS
c
c
       H2S04/GM
       0.00164
       0.00327
          00'(91
          00633
          00819
          009b2
          0 11 'i 6
          0131 0
          0 14 7 3
          01637
          02046
          02456
          C2S6f>
       0. n * ° 7 A
       0.03684
          t)4'093
          04502
          04912
          05321
          05730
          06139
          06549
          06958
          07367
          07777
          Gt. 186
          00003
          09823
          10642
          11460
          12279
          1 J09H
          13916
                         RATE,  GMS  H2SL'4/f,H C-
  00208
  00146
  00109
  00092
  00081
  00073
  00067
  00062
0.00059
0.00053
  00050
  OOC48
                                            0,
                                            0.
                                            o.
                                            0.
                                            0.
                                            0.
                                            0,
                                            0.
                                            0,
                                            0
                                            0
                                            0
  00047
  00046
  0004-6
  00046
  00045
  00044
 .00044
 .00043
 .0004-2
0.00041
0.00041
0.00040
0.00018
 .00016
 .00035
 .00033
 .00031
 .00029
 .00027
                                            G,
                                            0,
                                            0,
                                            0,
                                            0,
                                            0.
                        wnsivACo
                        -5.844 5 4
                        -6
                        -6
                        -6
                        -7
                        -7
                        -7
                        -7
            0. 14735
                                       G.OC025
                                                                 . 5 L 5 I. 5
                                                                 .80393
                                                                 .96862
                                                                 .09522
                                                                 . 19619
                                                                 .27076
                                                                 .34 320
                                                                 .39210
                                                                 .48165
                                                                 ,52464
                                                                 .55394
                                                                 . 'i S f Q ')
                                                                 i 56422
                                                                  36082
                                                                  5 5735
                                                                 ,55398'
                                                                  55920
                                                                  53384
                                                                  56131
                                                                  56713
                                                                  5 7 3 1 'j
                                                                  57916
                                                                  37570
                                                                 39222
                                                                 60598
                                                               7.62076
                                                               7.63690
                                                               7.65407
                                                               7.68575
                                                               7.72037
                                                               7.77396
                                                               7.81827
-1,
-7.
-7.
-7.
-7.
-7.
-7,.
-7.
-7.
-7.
-7.
-7.
-7.
-7.
-7.
-7.
-7.
                                        42

-------
CARBON C - 71 - 23
RUN NUMIJHU =  152- G     5  14  71
         RT = 300. OEG  F
TuTM. FLOW KAIt -  1000.0  CC/MM

i>I: KIT NT CO? =   11.3
I'LKCI. HT  U2 =    2,0
\'( :<(,! fU 1120 =   10.0
Cn^ClliJTRATION
co\ceiMri
-------
CAW-OV! C-7-1-23

RUN WUMbEK    r;3-«     5 10 71
TKMPJ''.KATURl!:  - IbO.  DEF J'1
TOTAL
          M  RAT I:
1000.0 CC/C. I
(•I.RCr;;l C02
       I   (//
       l H2U
CO'JCLMKAI I(H(
CIWU'NfRATION
                 11.3
                  2.0
                 10.0

              .SO?  --- 2000.0 PPM
               I JO  =   150.0 f'PK
tMRCKNI 112 504  -   61.24
SAUiRATU) LOADING -   0.3)i !,KS  II2S04/1,,
   GMS H2SU4/GM
       0.00612
       0.007 iO
       0.
         .00(JO /
         00 9 8 0
         0110?
         0 1 'J 3 1
         01837
         02 I 'i*
         024 !>0
         027!>6
         03062
         03368
         01674
         03-^81
         04287
         04593
         04099
         0520^
         05512
         06124
         06736
         07349
         07961
         08') 74
         091(16
         0979(1
         10411
         11023
       0. 11636
       0.12248
         13473
         15922
         17147
         1837?.
         19597
         20822
         22046
         23271
         24496
         26946
         2bi 10
         29J95
         30(>20
         311140
         33070
                         KATl;,  GMS
      0.34294
                112 SI I'. /(•,;•; C-.-11.J
                    0.01 /HI
                    0.0109 7
                    O.Ol-i I 3
                    0.01202
                    0.010*8
                    0.00962
                    0.00671
                    0.00439
                    0.00341
                    G. 002/6
                    0.00246
                    0.00220
                    0.00207
                    0.00201
                    0.00196
                    0.00192
                    0.00188
                    0.00185
                    0.00102
                    0.00179
                    0.00176
                    0.00174
                    0.00170
                    0.00166
                    0.00161
                    G.00 157
                    0.00103
                    0.00140
                    0.00144
                    0.00138
                    0.00134
                    0.00129
                    o.ociia
                    O.OClOd
                    0.00097
                    0.00087
                    0.00070
                    0.00064
                    0.00054
                    O.OOO46
                    O.i>0033
                    0.00033
                    O.OOU2U
                    0.00020
                    0.0"023
                    0.00021
                    0.90019
                    0.0001 I
                    0.00010
                    O.Q0014
wf. STVAL'l)
- .(i I 1)9
  ,117/8
  ,2 56'> 2
                                                             .61166

                                                             . 37(140
                                                            5.6221/
                                                              ,91340
                                                              ,01221
                                                              ,011960
                                                              , 10691
                                                              , I X IH f
                                                              . 13417
                                                              , 14532

                                                              , 16207
                                                              . 16740
                                                              , 1746b
                                                              ,17869
                                                              ,IB 346
                                                              , lbU4ti
                                                              . 19369
                                                           -6. 19919
                                                           -6.21491
                                                              22501
                                                              24090
                                                              25291
                                                              26564
                                                              ,30348
                                                              34157
                                                              39 166
                                                              ,40090
                                                              ,52975
                                                              62742
                                                              72976
                                                              .82285
                                                              .92790
                                                              .992 76
                                                              ,03374
                                                           -7.06207

                                                           -6.99403
                                                           -6.93017
                                                           -6.8H200
                                                           -6.7 J429
                                                           -6.02802
                                  44

-------
     CAKI'.UN C - 71 -  23
 c;
 c
 c
 c
 c
 c
c
c.
c
c
c
RUN UUMNCK - 157- G 53171
TLMPtRAlURE - 200. DEC F
TOTAL FLOW RATE
PIHCCMF C02 =
PlUCRiT 02 =
PLRCCNT 1120 =
= 1000. 0
11.3
2.0
15.0
CC/MIM

      COMCC.NTRAFICJN SU2 = 2000.0  PPM
      CCMCENTRAF IUM  M'J =  150.0  PPM
PERCENT H2SU4 =  67.91
SATURAFtD LOADING =   (
                      3a  CMS H2S1K/CM C
CMS
H2S04/GM
0.00272
0.00407
    0
    0
    0
    0
    0
    0
    0
    0
    0
    0
    0
    n
    0
    0
    0
    0
    0
    0
    0
    0
    0
    0
    0,
    0,
    0,
    0.
    0.
    0,
    0.
    0.
    0,
    0,
    0.
    0.
    0.
    0.
    0.
    0.
         00679
         0095).
         0 1 0 B 7
         01222
         01358
         01698
         02*037
         02377
         02716
         n '} 0 5 6
        .03735
        .OA075
        ,0441 A
        ,04754
        ,05093
        ,05433
        ,05772
        .06112
        ,06451
        ,06m
         07470
        ,08149
         Oot>2«
         09507
         10106
         10o66
         11545
         12224
         12903
         13502
         14940
         16298
         17657
         19015
         20373
                         RATI-,  GKS
            0.217J1
H2SU4/GN C-MIN
   0.00522
   G.00393
   0.00253
   O.UC 14 i
   O.OC. 129
   0.0012 3
   0.00119
   0.00116
   0.00114
   .0.0011 I
   C.00110
   0.00110
   0.00109
   0.00108
   0.00107
   0.00106
   0.00104
   0.00104
   0.00103
   0.00102
   0.00101
   0.00 100
   0.00099
   0.00098
   0.00097
   0.00094
   0.00091
   0.00089
   0.00086
   0.00064
   0.00081
   0.000/9
   0.00076
   0.00074
   O.OOC72
   0.00069
   0.00065
   0.00060
   0.00055
   0.00050
   O.OU045
WtiiTVACO
-5.24744
-5.52946
-5.96490
-6.53302
-6.63047
   67310
   /Ol'jO
   72538
   73860
   75807
   75456
   75094
   74733
   74963
   14 •> ^ 3
   74026
   75064
   74 678
   74292
   74530
   74135
   74377
   74624
   74210
   74461
   74988
   7 5 5 3 4
   76109
   76 7 Ib
   7/35 5
   78040
   78756
   79516
   79447
   79364
   7«253
   78006
   78802
   80883
   83352
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       -6
                                                       *~ 6
                                                       -6
                                                       -6
                                                       -6
                                                           -6.86298
                                      45

-------
     CARBON C - 71 - 23
rr
I
KUN Nuc.ubk =   150 - G    6
1 t-r.PtRATURC =  300.  OCG F
                            I 71


TLTAL FLOW  RATE  =  1000.0 CC/MIN
I'LRU.NT
              coz =
               U2 =
              1120 =
r
i.
CONCENTRATION
CL,'MCI:NTRATION
                 ii.3
                  2.0
                 10.0

               502  =
               NO  =
                           500.0
                           150.0
                     PPM
                     PPM
PH
               139/2
                              RAJ Cr  GMS
            0. 14748
                                   II2S04/GM C-MIfJ
                                      0.00054
                                      0.00043
                                      0.00037
                                      0.00034
                                      0.000 52
                                      0.00030
                                      0.00024)
                                      0.00027
                                      0.00026
                                      0.00025
                                      0.00022
                                      0.00020
                                      0.00019
                                      0.00018
                                      0.00017
                                      0.00016
                                      0.00015
                                      0.00014
                                      0.00013
                                      0.00013
                                      0.00012
                                      0.00012
                                      0.00012
                                      0.00011
                                      0.00011
                                      o.ooou
                                      0.00010
                                      O.OOU09
                                      0.00009
                                      O.OOOOb
                                      0.OOOC8
                                      0.00007
                                      0.00007
                                      O.OXi()06
                                      0.00006
WEST VAC C)
-7.52013
-7.74602
-7.89637
- 7.97176
-8.032/9
-8.08846
-8.13 ('til
-8.18400
-8.224/6
-8.26730
-0.35452
-8.43005
-8.49792
-8.55121
-d.60'459
-8.65286
-8.69480
-8.73411
-8.77080
-0.79036
-8.82677
-8.85154
-8.87019
-8.69036
-8.91077
-8.9 3 280
-8.9646-.I
-9.00770
-9. 03 til 7
-0.0/048
-9.10688
-9.13622
-9. 16838
-9.20501
-9.24431
                                         46

-------
     CARBON C - 71 - 23
 c

 C

 C

 C
RITJ NUMBER =  160-6     6   971
ThMPtRATURE = 200.  DEC  F

TllfAL FLOW KATE = 10UO.O CC/MIN

PtRCFNT CC12 =   11.3
PC-vCENT  02 =    2.0
PLUtUNT H2U =    5.0

COJCtNTKAl ION S()2 = 2000.0  PPM
CONCENTRATION  NO =   150.0  PPM

PLKCL-NT' H2Sei4 =  80.42
SATURATED LOADING- =   0.36. QMS H2S04/GM C
         GMS
 C.


 C
       0.
       0.
       0,
       0.
       0.
       0.
       0.
       0.
       0.
       0.
H2SH4/GM
0.00322
  ,00483
  ,00643
  ,00804
  ,00965
  ,01126
  ,0120?
  ,01448
  ,01608
  ,02010
  ,02413
0.02815
0.03217
0 * V -> O 1 )
0.04021
0
0
0
0
0
0
0
0
0
0
0
0
0.
0.
0. 12063
0.12867
                         RATE,  GMS
               04825
               05227
               05629
               06031
               06 A3 4
               •06 in 6
               072 3«
               07640
              00846
              0965IJ
H2S04/GM C~M(,\i
   0.00306
   0.002L5
   0.00 152
   0.00 110
   0. OU09<*
   0.0 (.!•() U 3
   C.OC073
   0.00067
   0.00061
   0.00054
   0.00050
   O.ooo4y
   0.00047
   0.. 000* 6
   0.00045
   0.00043
   0.00043
   0.00042
   0.00041
   0.00040
   0.00039
   0.00038
   0.00037
   0.0.0037
   0.00036
   0.00035
   0.00035
   C.00034
   0.00033
   0.00033
   0.00033
wtsrvAcn
-5.78171
-6. 12897
- 6 . 4 7 1 4 (5
-6.78822
-6.94636
-7.06719
-7. 18421
-7.26979
-7.35121
-7.47732
-7.52672
-7.54711
-7.56841
-7. 590'-9
-7.59632
-7.62014
-7.62645
-7.63295
-7.63965
-7.64658
-7.67393
-7.68174
-7.67922
-7.67665
-7.6648 \
-7.67960
-7.6741 I
-7.66832
-7.6503J
-7.63169
-/.60020
r
V
                                       47

-------
      Kin  I.'UI'BI i'. -   lol -  (i     6  10  VI
      I b ,'•'»•' IfRMUUl. -  200.  OLG  f:

      TUf/.i.  FLO< KMC- = 1000.0 CC/MIM
PffKCl. IjT
               (.02 =
                U2 -
               1 1 20 =
                 11.3
                  2.0
                 10.0

               S02  =  2000.0 PPM
                NO  =•  300.0 PPM
      Pt:RCTNT  II2S04 =  73.03
      SAl'UKATtrO LOADING -   0.3U  CMS  H2S04/GM C
      CO'.'CI'NTKAT
X, GMS H2SU4/GM  C
                               KAIF:
                02191
                02^56
                02921
                03286
                O^'-'^l
                04 OU
                04332
                047^7
                05)112
                   77
 O.I
 0.00730
 0.00876
 0.01022
 0.0116B
 0.0131 5
 0,
 0,
 0.
 0.
 0.
 0,
 n
 0.
 0.
 0.
 <•>.
 0.
 0.
 0.
 0,
 0.
 0.
 0.
 0.
 0.
 0.
 0.
 0.
 0.
 0.
 0.
 0.
0.
0.
0.
                0620o
                06573
                06938
                07303
                08033
                08764
                09494
                10224
                12413
                I 3 1 4 'j
                13876
                14606
                1606 /
H2S04
   P.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   C.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
   G.
   0.
   C.
   0.
   0.
   0.
   0.
   0.
   0.
   0.
                                         /GI" C-MIN
                                         001J97
                                         00429
                                         00308
                                         OOlVil
                                         0012!>
                                         0010'j
                                         0009S
                                         00087
                                         00084
                                         00081.
                                         000/8
                                         00076
                                         00075
                                         00074
                                         000/3
                                         000/2
                                         00070
                                         00070
                                         00070
                                         00069
                                         00069
                                         00068
                                         OOCiSU
                                         00067
                                         00067
                                         00066
                                         0006^
                                         00064
                                         00062
                                         00062
                                         OOU60
                                         000-j')
                                         000^7
                                         qOU'>6
                                         00054
                                         00049
                                         00045
                                         00040
h'FSTVACU
-5. 11272
-5.44042
-5.76707
-6.20578
   .66451
   .83348
   ,93254
   .00929
   .03945
   ,07388
   .09138
                                                               -6
                                                               -6
                                                               -6
                                                               -7
                                                               -7
                                                               -7
                                                               -7
                                                               -7. 10956
                                                                   10892
                                                                   11809
                                                                   1274'3
                                                                   126 •'j 6
                                                                   13672
                                                                   1 3634
                                                                   12530
                                                                   12467
                                                                   11338
                                                                   11262
                                                                   10107
                                                                   10026
                                                                   09933
                                                                   OU626
                                                                   07283
                                                                   07029
                                                                   06751
                                                                   05278
                                                                   04942
                                                                   04600
-7,
""" I i
-7,
-7.
-7,
-7.
-7.
-7.
™* I «
-7.
-7,
-7,
-7,
-7,
-7,
-7.
-7.
-7.
-7.
-7.
                                                               -7.04239
                                                               -7.03858
                                                               -7.04811
                                                               -7.06938
                                                               -7.09426
                                                               -7.14204
i.
                                        48

-------
CARBON C - 71  - 23

RUM  NUMUI-'R  =   16? - G    6
Tfcl-'PtKATURi: =  200. DFG  F
                             11  71
TUT/VL FLOW  RAl'K =  1000.0 CC/MI.N
(
(

(

(

(


(


(


(


(


(


C


(


(


(


(


(


(

•
C


f
V
. PL'0 7
-5.97719
-5.99394
-6.00188
-5.91142
                                    49

-------
      CARBON C  - 71 -  23
(

c

(

(
(
(
(
HUN NUK1U k  =
TLMJI;UAIIMI:  =
        161 - G
        200.  DC-G
                              b  14  71
TOTAL FLCW  RATH  =  1000.0 CC/f'IM

I'LRCErjT C02  =    11.3

PERCENT H20  =    10.0

CU\CK*TRAT10'J  Sl)2  =  2000.G PPM
C OX: t-iNTRAT I ON  Nf!  =    50.0 PF'M
PIRCLUT H2SU4  =   73.33
SATURATED LOADING  =
   3HS
II2S04/GM
0.00147
0.00293
0.00440
0.00587
0.007',3
0.00880
  01027
  01 173
  01320.
  01467
  01833
  02200
  02567
  02933
  03300
  03666
  04033
  044 00
  04766
  05133
  05500
  05866
  062 )3
  06600
  06966
  07333
  08066
  08800
  (19533
            U. 1 0266
              ,117*3
               12466
               13199
               139)3
               14666
               1 ft m
       0.
       0.
       0.
       0.
       C.
       0.
       C.17599
       0.19066
       0.20532
J
0.38 GMS M2SD4/GW C
RATI-, GMS H2SU4/OM C-,^IN
0.00305
0.00 f. 5 1
0.00205"
0.00166
0.00137
" 	 0.00126
0.001 18
O.OC1 12
0.00107
0.00104
C. 00096
O.OC092
0.00091
0.00009
0.00089
0.00088
O.OOOfcS
	 0.00007
0.0(>087
O.OOOrf?
0.00086
0.00035
0.00084
	 0.00084
0.00083
0.00082
O.OOOH1
0.00079
0.00077
0'. OOU75
0.00073
0.00072
0.00070
o.ooooa
0.00066
0.00064
O.OC059
0.00055
0.00050

WL-STVACll
-5. 7U759
-5.97820
-6.17923
-6. 38323
-6.57505
-6.65564
-6.71235
-6. 75963
-6.802«0
-6.83 387
-6.89-795
-6.92697
-6.93275
-9.25706
-6=936 5 b
-6.93434
-6.92778
	 -6.92112
-6.91444
-6.90758
-6.90496
-6.9022(3
-6.89956
-6.89677
-6.8894 3
-6.1; 9 094
-6.8';i495
-6. H7870
-6.8 1, 1 1> (-,
-6.87502
-6.87803
-6.87094
-6.87399
-6.86639
-6.H6948
-6.S7288
-6. 85029
-6.88884
-6.91364
                                            0.00044
                                                                  -6.94325
                                        50

-------
     CARBON C - 71 -  23
(
c
RUM NUf-'WER
  164 -
= 200. DEC  F
                              6 15 71
   '  TOTAL  FLC'fc RATE =  1000.6 CC/MIN
PtRCENF C02 = 11
I'tRCtM 02 = 2
PIKCt-NT H2U = 10
CUNCtNTRATtQN S02
CL'JChKT RAT tOU .\C5
PfcRCEI-JT "H2SU4 =" 7
SATURATED LOADING
X, GMS H2S04/GM C
0.00146
0.00292
O.C0439
0.00585
0.007U
0.00877
0.01023
0.01 170
0.01316
0.01462
0.01827
0.02193
0.02553
0.02924
0.032B9
0.03655
0.04020
0.04386
0.04751 '
0.05117
0.05482
0.05848
0.06213
0. 065 79
0.06*) 4 4
0.07310
6.0b04l
0.08772
0.09503
0. 10234
0.1C965
0.11696
0.12427 """
0.13158
0.13889
0.14620 '
0.16092
0.17544
.3 • ••• . .
.0
.0
= 1000.0 PPM
= 15C.O PPfo
3.10
= 0.38 GMS II2S04/GM C
RATF:, GMS U2SU4/GM C-MI.V
0. 00 181
0.00 12 '3
" 	 '' 	 : "" '0. 00031.
0.00071
0.00066
0.0006^
0.00060
0.00059
0.00057
0.00057
0.00054
0.00054
0.00052
0.00051
"" 	 " 	 "0.00051
0.00050
O.OOC50
0.00050
0.00050
0.00050
0.00050
0.00050
0.00050
	 0. 00050
0.00050
O.OOU50
0.00049 	 	
0.00048
0.00048
0.00048
< • 0.00 04 7
''..' O.C0047
V ' : 	 " 0.00046
G. 00045
0.00045
O.OOU43
0.00042
' 0.00040




WHSTVACU
-6.3093.5
-6.67460
- 7 . 1 0 3 J 3
-7.23667
-7. 30837
-7. 36403
-7. 3ti447
-7.40551
-7.42717
-7.43624
-7. 46659
-7.47022
-7.488L3
-7.49215
-7.49627
-7.49306
-7.48236
'-7.47898
-7.46805
-7.45700
-7-44582
-7.43451
-7.42308
-7.4115?
-7.39982
-7.38793
-7.37891
-7.36947
-7.34414
-7.33366
-7.32272
-7. 30328
-7.2831.2
-7.27038
-7.25704
-7.26015
-7.23066
-7.21668
                                         51

-------
                      APPENDIX    A-3






COMPARISON OF WESTVACO MODEL TO EXPERIMENTAL SORPTION DATA
                          52

-------
                   RUN NUMBtR
                                  139
                                            4  22  71
Ul
U>
      RATECt I )  = COEF *
            WHERE COEF =
                POKfcR »
                   XS =
                 YS02 =

 XUl.GMS H2S04/GM C

        0.00294
        0.00441
        0.00539
        0.00736
        O.OC8B3
        0.01030
        0.01177
        0.01324
        0.01472
        0.0183-}
        0.02207
        O.Q2575
        0.02943
        0.03311
        0.03679   "
        0.04047
        0.04415
        0.04783
        0.05151
        C. 05518
 "   '-    0.03336
        0.06254
        0.06.622
""" .....  0.06990
        0.07353
        0.0*094
                                          (l.-XIIJ/XS)  * 
-------
  RUN NUMBER
                          4 23 71
      KATECtI) *
_XU > tGMS H2S04/GM

        0.00292
        0.0043?
        0.00583
        O.OCU21
        0.00875
        0.01021
        0.01167
        0.01312
        0.01453
        0.01323
        0.02167
        0.02552
        0.02916
        0.03281
        0.03645
        0.04010
        0.04375
        0.04739
        0.05104
  •      0.05468
        0.0r)333
        0.06197
__.	 .  0.06562
        0.06926
        0.07291
        O.OK020
        0.OK 749
        0.09478
	0,10207
        0.10936
        0.11666
	._    0.12395
        0.13124
        0. 13853
        0. 14582
        0.16040
        0.17498
OEF * tl.-Xin/XS) * 
-------
                   RUN NUMBER  =   141
                                            4 26 71
Ul
      RATECt I I = CGEF *
            WHERE COEF =
                POwtR «
                   XS =
                 YSOZ =

 X( I J ,GHS H2S04/GM C

        0.00148
        0.00296
        0. 00444
        0.00592
        0.00740
        O.OUSBS
        C.C1C36
        0.01184
        O.C1332
        0.01430
        0.01850
        0.02220
        0.02590
        0.02960
        0.03330
        0.03700
        0.04071
.....    0.04441
        0.04811
      * 0.05181
        0.05551
        O.C5921
        0.062V1
                                          (l.-Xtn/XS) * 
-------
                   RUN NUMOtR
                                            4 27 71
                              i)  =  cotF * (i.-xm/xsi
                              WHERE COEF =   0.01050
                                  POr-ER =   0.40500
                                     XS =   0.33000
                                   YSU2 =   0.00100
                              * (YS02»**POW£R
Ui
                  XU >,GMS  H2S04/GM  C
0.00144
0.00285
0.004J1
O.C0575
0.00719
0.00963
0.01006
C.01150
O.C1294
0.01438
0.01797
0.07156
0.02516
0.02875
0.03235
0.03594
0.03953
O.C431 3
0.0^.672
0.05032
0.05391
O.OD750
0 . U
-------
                           RUN h'JMBER =  133 -G
                          4  21  71
                          RATEC(il= COEF * (l-XUI/721 * Y2C2«*.4I *-(Y02**.63)
                             WHERE  COEF= .000159 * EXPt 552CM I/ t T *460) ))
                                     XS=   0,38000         T= 200.00000
                                       =	D.00200	YUZ=	Q.00700__
                                                       * (YH20**,73)
Ul
YH20= O.I 0000
XI! ) |G«S H2S04/GH-C 	 RAT£_,_GMS. H2SOW.SH._C-HIN. ,_._CALCULATtU RATE, GKS H2S04/GH. C.-M]
0.00145 ' 0.0024220 0.0004622
0..00290 O.OC17S13 O.OC04604
0.00435
0.00530
o.nn7?s
0.00870
0.01015
0.01160 .
0.01305
0.01450
O.OlBil
0.02175
0.02538
0.03263
0.03625
0.04351
0.04713
0.05438
0 . OS50 1
O.OM63
0.06526
0.06888
0.07251
0.07976
0.08701
0. Q9426
0.10151
0.10876
0. ) IfrO? 	
0.0012296
0.00-58421
0.0005291
0.0005068
0.0004918
0.0004S44
O.C004770
0.0004546
0.0004397
0.0004173
0.0004099
0.0003913
0.0003875
O.OC03763
0 * CCO^ "* °6
0 .fOO 3^^9 ,,. .
O.U003689
0.0003652
O.OCC3iM5
O.OU03577
0.0003540
0.0003540
0.0004587
0.0004569
0.0004551
0.0004534
O.OC04516
0.0004498
O.OOC44BO
0.0004463
0.0004418
0.0004374
0.0004330
0.0004286
0.0004241
0.0004197
O.OC0415i
O.COC4109
0.0004064
0^0004D?0
0.00039f6
0.0003932
0.0003643
0.0003799
0.0003666
0.0003577
0.0003400
0.0003312
n.nom??*
IN 	 .UIFFd.J.
0.0019598
	 0.0012908 ...
0.0007710
0.0003U52
0.0001634
O.CC00757
0.0000552
0.0000420
0.0000363
0.0000307
0.0000202_
0.0000171
0.0000067
0.0000038
0.0000068
O.OOC0098
0.0000166
0.0000196
0.0000189
0.0000219
O.OC00213
0.0000205
0, DODO 199
O.OOC0154
0.0000147
0.0000)0"*
0.0000051
0.0000000
0.0000140
0.0000228
. . D. 0000279.. _
KEAN DEVIATION =   0.0000186    ROOT  ,".EAN  SOUARE  DEVIATION
RESIDUAL-SUK-OF- SdUARES _=_U.U850E--0-^	
KEAN PERCENT DEVIATION  =    4.484&6H
                                                                                         0.0000222

-------
                   KUN NUMbtR
                                  143
                                            4 28 Tl
Ul
oo
                       KATEC< I )  = CtJEF *
                              HHtRE COEF =
                                  »0*ER =
                                     xs =
                                   YSUZ =

                  XII) ,OM'S  H2S04/GM C
0.00145
0.00290
O.OC4J5
O.C0580
O.O0724
O.C'C869
O.G1014
C.01159
O.U1304
0.01449
0.01811
0.02173
0.02536
0.02898
0.03260
0.03622
0.03985
0.04347
0.04709
0.05071
0.05434
0.05796
0.06158
0.06520
0.06883
0.07245
O.OT969
0.08694
0.00413
0.1014?
0. 10867
0.1159?
0.12316
0. 13041
0.13765
0.14490
0.15939
                              * (YS02)**POKER
                    0.01050
                   0.40500
                   0.-.3QOO
                   0.00050

                 RATE,  G.XS H2S04/GM C-MIN   CALCULATED RATEt CMS H2S04/GM C-HIN
0.0033683
0.0021586
0.00105C3
0.0008330
0. CCC6990
0.0006157
0.0005577
0.000521&
O.OOC4962 	 	
O.OOC4817
O.COD4745
0.0004636 ~ ~~ ~ '
O.CC04564
O.CC04527
O.OCC445i>
0.0004382
C, 0004346
0.0004310 	 " ~- " ' •-"- 	
O.OCC4238
0.0004201
0.0004165 	 " " 	 "
C. 0004129
O.OOC4093
0.0004056
0.0004020
0.0003984
0.0003948
O.D003875
O.CGC3S03
C. 0003730
0.0003658
0.0003586
0.0003477 	 "
0.0003404
0.0003332
0.0003223
0.0003006
0.0004815
O.OOC4797
0.0004773
0.0004760
0.0004741
0.0004723
0. 0004705
0.0004636
0.0004663
0.0004649
0.0004603
0.0004557
0.0094511
0.0004465
O.OOC4419
0.0004373
0.0004327
O.C0042B1
O.C004235
0.0004189
C.C004142
0.0004096
0.0004C50
0.0004004
0.0003958
0.0003912
O.OG03820
0.0003723
Q-.C003636
0.0003543
0.0003451
O.C003359
0.0003267
O.C003175
0.0003033
0.0002990
0.000.2806
    DIFFtI »

0.0025368
0.0016789
O.OOC5725
O.OC03570
0.0002249
0.0001434
0.0000873
0.0000530
0.0000294
C.OOOOIS3
0.0000142
0.00000^9
0.0000053
0.0000062
0.0000036
0.0000010
  .0000020
  .0000029
  .0000003
  .0000013
O.OOC0023
O.OOC0033
0,0000042
0.0000052
0.0000062
0.0000072
C.C000128
0.0000148
0.0000167
0.00001.87
O.OOU0207
O.C000226
0.0000210
C.0000230
O.CC00249
0.0000233
O.C000200
                                                                                                             0.
                                                                                                             0.
                                                                                                             0.
                                                                                                             C.
                  MfcAN DEVIATION =
                                      0.0000154   ROOT MEAN SQUARE DEVIATION
                                                                                  0.0000231

-------
 RUN  NUMBER »   139 -G
•, 22 71
RATtC(l)= CCCF  *  U-XU)/72I * Y202**.4I  *  (YQ2**.63)
        COEF=  .000159  » EXPI5520*(t/• ,;•..'"
0.0006791
0.0006755
n.onnAAfu
0.0006610
0.0006538
O.OOO^'tf.'i
0.0006356
0.0006247
n.nonhiTH
0.0006028
0.0005883
fi-or>ns77i
0.0005484
0.0005230
n.nnrx.od^
ROUT MEAN .SQUARE DEVIATION =
L5155E-06 	 	 . , 	 .-.„ -

_.RAT£t .GHS_H2SQ'./CM.C.-MIN ._
0.0008920
0,0008885
0.0008850
0.0008815
0.0008781
0.0008746
0.0008711
0.0008676
0.0008641
0.0008554
0.0008467
o.oooaiao
0.0008293
0.0008206
o.oooai 19
0.0008032
0.0007945
0.000/858
0.000/771
. .0.0007684 	 	 , 	 	
0.0007597
0.0007510
O..OO.C.7A2? .. - 	 	
0.0007336
0.0007249
0. 000/075
0.0006901
0.0006727
0.0006553
0.0006379
0.0006205
O.OOOftOiO
0.0005856
0.0005682
n.oons5on
0.0005160
0.0004812
0..0004.46'. _. 	 _ 	
0.0000678

	 DIFF.(.U_
0.0061682
0,00 ',220 I
0.00211775
0.0012467
0« 0004076
0.0002004
0.0000/31
O.OOOCO'.O
0. OOU0434
0. 0000055
0.0000841
0.00001)99
O.OOOOHH5
0.0000870
0.0000(J'..5
0. 00001!', 1
O.OOOOH27
0.0000t;12
0.0000/62
. 0.0000/48 	
O.OOU0697
0.0000646
0,OOnoS95
0.0000544
0.0000494
0.0000392 __
0.0000291
0.0000109 :
0.0000008
0.0000023
0.0000042
0.00001Q8
0.0000172
0.0000201 :
_0.0000266_.. ..
0.0000324
0.0000418
0..000043.9-,.. -

                                                59

-------
   RUM KUMttER »

  RATECd )=  COCF
     WHERE COEF=
             XS =
                140-G
•> 23 71
                * (l-X(I)/72)  *  Y202*<'.4) * (Y02**.63>
                .000159 * EXP(5520*( 1/i T f'.60 )))
                  0.38000          T=  200.00000
                                 Y.()2~	.O.r.020.0.0			
                              *  (YH20**.73»
	.YS02-	0.00250	
.           YM20=    0.10000

., Xt 1 1 ,GMS II2S04/CH.C	RAJE->._.GHS-H2S04/_GI>UC.-M1N	CALC.ULAT.CO
                                                                      C«S._N2SO't/CM..CrHl.N..
                                                                      .OIFFd.l.
0.00292
	 0.004J7 _..
0.00583
0.00729
0.00875
0.01021
0.01167
0.01312
0.01458
0.01823
0.02187
0.02552
0.02916
•0.03281
0.03645
0.04010
O. 04 37 5
0.04739 '
0.05104
- - 0*05468 	
0.05833
0.06197
0.06926
0.07291
0.08020
O.;08749
0.09478
• -0. 10207 —
0. 10936
0.11666
	 0.-12395,. _
0. 13124
0. 13853
0. 14*8?
0.16040
0.17498
0.0045633
__.. 	 	 0.0032855 	 _.„ 	 . 	
0.0015552
0.00.12923
	 0..001131.7
0.0010258
0.0009638
0.0008907
0.0008433
n.orinn;>';o . ..•_.
0.0008141
0. 0008031
0.0007849
0,0007776
0.0007630
0.0007557
0.0007447
0.0007374 : : . '
Oi "'10 7^*1
0.0007265
0.0007223
0.0007119 ..„. -,
0.0006972
0.0006899
, „- , . „ 0.0006827 -' ' •., •
0.0006717
0.0006608
0.0006461
0.0006352 .:'• :
0.0006206 . / •• ' •":..• .1 . . .• .
	 ... 	 	 _. o.000'-0q7 ' • :
0.0005804
0.0005513
0.0009753
	 0.0009716.... 	 	 	
0,0009678
0.0009640
0.0009603
0.0009565
0.0009527
0.0009489
O.OC09452
0.0009357
_ 	 0.0009263 „_
0.0009169
0.0009075
, o.oooagno
0.0008886 .
0.0000792 • ..'.;;'
0.0008603
0.0008509
.. .. 0.0008414 	 	
0.0008320
0.0008226
0.0008037
0.0007943
0.0007566
0.0007377
0.0007000
0.0006811
0.0006434
0.0006246 . .;' .,;•...:
0.0005680
0.000530J
0.0035879
.. 0.002 3 140.
O.OOO'JU/'i
0.0001715
0.000069',
O.OOOOU1
0.0000326
0.000054373
0.0000052
0.0000773
0.0000715
0.0000635
0.0000593
0.0000478
0.0000362.
0.0000283
0.0000204
0.0000162
0.0000082
0.0000040
O.OOOQ04Q
0.0000124
0.0000210
MEAN DEVIATION  » .  0.0000620   ROUT  MEAN SQUARE DEVIATION
RESIDUAL  SUM  OF SOUAR6S '• 0.16349f,-0t                  :.  ,
MtAN PCRCENL-OEVUnON^=	8.0887070	...J	'.	
                                       0.0000715
                                                   60

-------
  RUN  NUMBER =  l'il-G
'( 26 71
 RATEC(l)*  COEF * (l-Xtl)/72)  «• Y202**.*) *  (Y02**.63) * — - . 0.096?!. ~
0.10361
O.U101
	 _ . 0. 118*?
1 0.12582
( 0.13322
0,1*802
6. 16282
--. — .. o. 17762
0.192*3 , ;
-- HFAN nrviAriritj A
0.0051 181
	 	 _ 0.00*2177
0.002319?
O.OQ11*15
. 	 	 .., 	 .0..000935J
0.0000359
0.00078*3
	 	 	 0.00075U 	 _ 	 	 	
0.000736*
0.0007253
	 0.0007217
0.0007106
O.OOOY032
. „ 	 , . . 0. 0006959
0.00068*9
0.0006/75
	 	 	 . Q. 0006/02.. 	 	 	 .
0.0006628
0.000655*
	 	 	 ..a. 0006*00.
0.0006*07

0.0006260
0.0006223
n.onrif.i/,9
0.0006038
0.0005928
0.0005671
0.0005523
0.0005192
0.0005008
0.000*8?3
0.000*6*0
0.000*23*
.0.0003*2*
.n.nooo??n. R£inr Mr-AU SQUARE .DEVIATION..".. ...
0.0007981
0.0007950
0.000/919
0.0007888
O.Q007056
0.0007825.
0.000779*
0.0007763
0.0007732
0.0007700
0.0007622
0.00075**
0. 0007*66
0.0007388
0.000/310
0.0007232
0.000715*
0.0007076
0.0006998
0.0006920
0.00068*2
0.000676*
0.0006686
0.0006608
0.0006530
0.0006*5?
0.0006296
0.00061*0
0.0005828
0.0005672
0.0005360
0.0005203
0.00050*7
0.000*891
0.000*579
0.000*267 	 „. .-
0.0003955
0.00003*9 	 	 _..
0.00*3200
0.003*2*7
0.0015278
0. 0003527
0.0001*96
0.0000') 3*
0.00000*9
0.0000251
O.COOOJ68
0.0000** 7
0.0000*06
0.0000*38
0.0000*3*
0.0000*29
0.0000*61
0. 0000*5 /
0.0000*5.4
O.OOOOV.9
0.0000***
0.0000**0
0.0000399
0.0000357

0.00003*8
0.0000307
0.0000303 .
0.0000257 .
0.0000212
0.0000166
0.0000157
0.00001*8
	 O.OOG01.76_
0.0000168
0.0000196
0.000022* 	
0.0000252
0.00003*5
	 ;. __0. 0000*01 	
0.0000531
 RESIUUAL  SUM OF SOUAIUS '  O.*023'.>(.-07
 MUN PERCENT DEVIATION  '    5.5525713
                                                  61

-------
    RUN NUMBER
                  142-C
27 71
   RATECU) = COEF * (l-XUI/72)  *  Y202**.4) * IY02**.63) *  (YH20+*.73)
      KHEKE  COEF = .000159 *  EXP ( 5520*< 1 / I T+460) ) >
              XS =   0.3BOOO          T=  200.00000
  	  ..._YSG2 = ....0.00100	Y02=___.. 0.02000							
            YH20=   0.10000
      ) iGMS.II2SO'i/GM C..
                          .RATE,  GMS-.H2S04/GM_.CrK IN....CALCULATED  RATet__GMS .JfZS04/CM_C.-.MIN._-
                                                                         ( )__.
0.00144
o.oo2aa
0.00431
0.00575
0.00863
0.01006
0.01 ISO
0.01294
0.014.18
.0.01717 	 	 	
0.02156
0.02516
0.02875 	
0.03235
0.03594
0.04313
0.04672
.0.. 05032 - , - - —
0.05391
0.05750
0.06469
0.06829
0.. 07 188 	
Of07907
0.08626
0. 09^44 t 	
0. 10063
0.10782
. 0»-1 1 501..,.. 	 	 , 	
0.12220
0.12938
0.13657
0.14376
0.15814
0. 17251 	 _.
0.0050370
0.0036017
0.0021J80
O.OP09639
0.0007573
0.0007067
0.0006740
0.0006559
0.0006522
_ . 0.0006414 	 ._ 	 	 ;. 	
0.0006341
0.0006233
....0.0006160 	 	 	 	 _ 	
0.0006088
0.0006016
0.0005943
0.0005070
0.0005798
0.00056U9
0.0005617
0.0005508
0.0005436
	 _0. 00 05400 	 . 	
0.0005290
0.0005182
0.0004965
0.0004055
	 0. 0004 74 7_ — 	 	 	 „,„ 	 „,
0.0004638
0.0004493 . v
0.0004204
0.0003914
.n.ooowi 	 	
0.0006787
. . 0.0006761
0.0006735
0.0006710
- ,-Q. 00066 84
0.0006658
0.0006632
0.0006607
0.0006501
0.0006555
..... 0.0006491.. 	 _• 	 	
0.0006426
0.0006362
0.0006297 . 	 ... _.
0.0006233
0.0006168
0.0006104
0.0006040
0.0005975
0.0005911
0.0005846
0.0005782
..0.0005717
0.0005653
0.0005589
	 0.0005524 	 , 	 „
0.0005395
0.0005266
0.0005009
0.0004880
	 Q. 00.0475 1 	 _, 	
0.0004622
0.0004493
0.0004364
0.0004235
0.000.3978
	 Q.. 0003720. . 	 _
0. 004.1 V>«3
0.0014644
0.0002929
0,0001651
0.0000915
0.0000434
0.0000134
0.0000022
O.OOOUOJ3
	 O..OOOOU/ 7..
O.OOOOOU5
0.0000129
_..._ 	 0.0000137.
O.OOOOi. 45
0.0000153
0.0000161
O.OUUOU-.9
0.0000177
0.0000149
0.0000157
0.0000165
o.nonnn?
0.0000145
0.0000153
	 	 O.OOO.OL24..
0.0000105
O.OOQ0085
0.0000044
0.0000024
	 0, 0000004_
0.0000016
0.0000000
0.0000016
0.0000032
0.0000064
	 ' ..0.00000.96..
  MEAN  OEVIATIOfJ ='   0.0000107   ROOT  MEAN  SQUARE DEVIATION
-. RESIOUAl. SUM 01- SOUAR£$-.-.-0.5792bE-08	^^	^		
  MEAN  PERCENT DEVIATION =   1.8736451
                                    0.0000135
                                                    62

-------
 RUN NUMBER =  143-G
'. 28 71
RATEC(I)= COCF * «l-X(I)/72)  *  Y202*».4)  * (Y02**.65)
   WHERE CGHI-- ..000159 *  fXP ( 5520* ( I/ ( T *460 ) ) )
           XS=   0.38000          T =  200.00000
   		Y.S02=..  0.00050....	Y02 =	0.0700Q	
         YH20=   0.10000
                              * 
X(I),GMS-H2S04/G.M. C 	KATJi. ..CHS  U2Sn4/GM_.C-MIN .. .CALCUI.ATCO .RATE,  CMS l!2SO't/GM .C-MIN.
                                                                      otpni
0.00145
0.00290 ... _ 	
0.00'i35
0.005BO
0.00724 . 	 ...._ ...
0.00869
0.01014
	 ......O.Q11S9 . .. 	 	 ...
0.01304
0.0l'i'.9
. 0.01811 	 	 	 ...
0.02173
0. 02536
	 	 0.02098 	 	 	
0.03260
0.03622
0 . 0 J9 B 5.
0.04347
0.04709
fi,n«,r>7 J
0.05434
0.05V96
0 m 0 O I *^ '}
0.06520
0.06C83
... _. . 0.07245
0.07969
0.0869't
ft ftG& 1 A
0. 10143
0. 10867
— - 0.11592
0.12316
0.13041
ft - 1 17/. K
0.14490
0*. 15939
0.0031683
.O..OQ21'JE6... 	 	 ... .
0.0010503
Q. 0008350
0.000699.0.., .
0.000615V
0.00055/7
.0.0005216. 	
0.000'i9()2
0.000481V
0.000'fY'iS. 	 , .
0.0004636
0.0004564
0.0004527 	 r 	 : 	 	
0.0004455
0.0004382
0.0004 Vi 6
0.0004310
0.0004238
0 ,no<1420'
0.0004165
0.0004129
f) .(Hift'.OO 1
0.000405h
0.0004020
!).0003984._ 	 	 	 _ 	
0.000394B
0.0003875
P.0003PO^
0.0003/30
0.0003650
O.OOO^ORh . 	 ,~- -
0.0003477
0.0003404
0 jO-10** '»?
0.0003223
0.0003006
0.0005143
0.0005124
0.0005104
0.000501)4
0.0005065
0.0005045
O.Q005025
.0.0005006
0.0004986
0.0004966
0.0004917
0.0004868
0.0004819
.O.C004769
0.0004720
0.0004671
0.0004622
0.0004573
0.0004523
0.00044/4
0.0004425
0.0004376
O..C00432&
0.0004277
0.0004228
0.0004179
0.00040)10
0.0003'K!2
o. 000.3 an j
0.0003785
0.0003687
0.0003500
0.0003490
0.0003391
0.0003293
0.0003194
0.0002997
0.0028539
0.0016462
0.0005399
0.0003246
0. OOd 19,° 5
0.0001112
O.U000552
0.0000210
0.0000024
0.0000149
O.OOCOJ 12
0.0000212
0.0000255
	 	 	 '0.000024a...
0.0000265
0.0000208
0.0000275
0.0000262
0.0000286
0.0000273
0.0000260
0 . 0 0 ^ n "^ f: 7
0.00(JO2i4
0.0000^21
0.0000208
0.0000105
0.0000133
0.0000107
O.U000081 ,
0.0000055
0.0000029
0.0000003
0.0000013
0.0000013
0.0000039
0,0000029
0.0000008
MEAN DEVIATION =   0.0000173    ROOI  HCAN SQUARE DEVIATION
RESIDUAL SUM OF SQUARES  * 0.13il7',t-07
MEAN PERCCNV DEVIATION =	3»941>U342-	
                                                                0.0000212
                                                63

-------
   HUN NUMBER
144-G
                              29 71
  RAUC(l)= COEF  »  U-XIII/72) * Y202**.4I  *  (Y02**.63)  * (YH2U**.73)
     KHE1E COCP =  .000159 » EXP ( 5520* (I/ ( T + 4iiO ) 1 )
              XS-    0.30000         T= 200.00000
		_  -_.YSn2=.	0.00200	VD2-.	0..03500			,	
           YH20*    0.10000

.. XII ),GHS. H2S04/GII C	RATE., -GHS..H2SX14/.GM C.-M1N—.GALCUI.ATCO.JlATEi .CMS  HZS04/GH_C_-MJ.N	OIFF(.I) .
0.00201
n.nn/.4n
0.00086
0.00/33
0-fWlRftf)
0.01026
0.01173
0.01320
0.01466
0.01833
0.02199
0.02566
0.02932
0.03299 	 _., 	
0.03665
0.0't032
. .0.04399 	 ___.
0.04765
0.05132
0.0^498
0.05865
0.06231
V.1 » VO'1 ^ tf -
0.06964
0.07331
0.08064
0.08797
0.09530
0. 10263 v , 	
0.10996
0.11730
-0.12463 	
0.13196
0.13929
0. 14662
0.16126
0.17594
0. 19061
0.20527
0.0053409
0.0037.517 ' -._...
0.0025259
0.001'>452
n.nnf/.?f>/.
0.0013558
0.0013001
O.OOIP518 	 - 	 - 	 	
0.0012035
0.0011367
0.0010995
0.0010810
0.0010698
	 0.0.010623.. 	 	 ,. 	 	
0.0010549
0.0010474
	 0 . 001 0400 	 '- 	 _._
0.0010326
0.0010252
O.OOlO?i5
0.0010178
0.0010141
Cf t r~. ™i \ tj P .', ,'„
0.0010030
0.0009992
n ,prnioiia
0.0009d4.3
0.0009769
n >OOOr)6S8
0.0009509
0.0009398
0. 0^09212
0.0008909
0.0008766
n.onog«i<,
-------
 RUN NUMBER =   K5-G
30 71
RATEC(I)=  COEF  *  ll-X(I)/72)  * Y202**.4) * (Y02**.63)
   WHERE COEF =  .000159 * EXP15520*f I/(T+460)))
           XS =    0.38000         1=  200.00000
                           * (YH20**.73)
YM20= 0.10000
Xlll.GHS. H2S04/GM.C. 	 RAIE
0.00290
_ ... 0.00436. 	 	 	 	 ......
0.005BI
0.00726
...0.00871 	 	 	
0.01017
O.OU62
0.01307 	 _ . .
0.01452
0.01815
	 0.02178 	 	 .
0.02541
0.02904
.0.03P6/ . ........
0.03630
0.03994
	 __ 0.04357 	 ...
0.04720
0.00083
0.05809
0.06172
0.06898
0.07261
0.07987
0.08713 •
0'.09439
0.10891
0.11618
0.13070
0.13796
	 	 0. 14522- 	 	 . 	
0.. 15974
0.17426
I...GMS H2S04/GM..C.-MIN
0.0064766
	 0.0051454 	 	 	
0.0037780
0.0026626
. _ O.d014752 	 	
0.0010650
0.00102ia
. 0.00099.! I
0.0009715
0. 0009 j I 9
... .0.0009031 . . _ 	 	
O.OOOH816
0.0008635
0.0008312
0.0008203
O.OOOfl(]9C,
0.00079U8
0.0007916
0.0007772
0.0007700
0.0007556
0.0007520
0.0007268
0.0007124
0.0006764
0.0006621
O.OO06405
0.0006225
0.0006009
_... 0 .0005793..-.. 	 -
0.000536?
0.0004893
...CALCULATED KATE. ..CMS.. H2SP4/GU C-HLN
0.0008921
„., 	 	 _ . 0,0008887
0.0006852
0.0008818
0.0008749
0.0008715
0.0008680
0.0008646
O.OOOU560
	 	 	 0.0000474. 	 	
0.0008388
0.0008302
0-000il?17
0.0003131
O.OOOH045
. 	 . 0.0007959
0.0007873
0.0007787
0.0007701
0.0007615
0.0007530
0 .OOO /<«'n4
0.0007358
0.0007272
0.0007100
0.0006928
0.0006757
0-0006505
0.0006413
0.0006241
0-0006069
0.0005U98
0.0005726
	 	 	 0 .0005554 	 ....
0.0005211
0.0004867
IHFFI I)
0.0055045
0.00'.,">66
0.002H928 	
0.001 HiOO
0.000'i969
0.0001VOI
0.000150'i
0.000 1 <")0
0.0001069
0.0000759
0.0000'i57
0.0000427
0.0000 "13 3
0.0000? 39
0.0000181
0.0.000159
0.0000137
0.0000115
0.0000129
0.0000143
0.0000157
0.0000171
0.000019B
0.0000248
0.00003L2.
0.0000340
0.0000368
0. 0000395
0.0000351
0.0000379
0,0000335
0.0000327
0.0000283
0..0000239.
0.0000151
0.0000026
MEAN DEVIATION  =    0.0000418    ROOT MEAN SQUARE DEVIATION -
RCSinUAL  SUM  OF SQUARIS  "  O.H287E-06
                                                              0.0000594
                                                 65

-------
 RUN  NUMOFR =  148 -G
          5  7 71
 RAteCtt)--  COEF
    WHERE  COCT=
            xs-
	 ..YS02 =
          YH20 =
* (l-XID/72) * Y202**.41  *  (Y02*».63)  *  tYH20**.731
.00015'* * EXP(5520*< l/IT + 460)JI
  0.38000         T=  150.00000
  0.00250	.Y02-^__.0.02000			
  0.10000
 XII 1 ,GKS  H2S04/GM C
                        RATE,..CMS II2SQ4/GM..OMIH    CALCULATE) RAf d-GMS-H2S04/GH. CrHtN	
o.oo,v9
0.00343
0.00'i')7
O.OCW2
0 006(36
0.00801
0.00915
0.01029
0.01144
0.01'i29
0.01715
0.02001
0.02287
0.025/3
0.02859
0.03145
0.03't 34
0.03717
0.04003
-0.04288
0.045/4
0.0'i860
0. OS 1 kf\
0.05432
0.05/18
0.06200
0.06862
0.07'.33
. 	 0.00005-
0.085J7
0.001'.9
OiC972l
0. 10292
0. 10864
0 1 1 'i 3 6
0.12580
0.13723
	 .0. 148&7-
0. 16010
0.17154
0. 1829U
0. 19441
0.20565
- 	 - 0.21728-
0.0216960
	 	 0.0199966. 	 	 	 	 - 	 	 	
O.Q1B43U8
0. 01/0509
n r(l IS71/J7
0.01'.47J'i
0.0133122
p,ni?2Ti9
0.0112162
0.008Y'.-20
0,n(u,y|?7
0.0051266
0. 0041636
0.00380LO
0.0035122
0.0032573
0.00''0'<07
0.0028324
0.0026908
0.00?^71N
0.0024755
O.OOZlU't^ '
« 0 . lr'r'
0.0004362
0.0003682
. .. _ .... . . ... Q.nPi"i xrmq
0.0019301
.. . 0.0019333 	 	 	 	 _.
0.0019274
0.0019215
0.0019156
0.0019098
0.0019039
0.0018980
0.0010922
O.OOUI775
0.001B62B
0.0018401
0.0018335
.0.0018108 ,. 	
0.0018041
0. 0017894
0.0017747
0.0017601
0.00174'J4
-.0.0017307 	 - 	 	
0.001*7160
0.0017014
rt f\f\\fftf"J
0.0016/nrv,QAO
0.0005166
0.0005259
0.0005Z95.-
C.EAN DEVIATION  =    0.0014892   ROUT MtAN SQUARC DEVIATION
RESIDUAL SUM OP SQUARES-=^0*2-9836l:-03	:	
MEAN PERCENT DEVIATION  =   47.7267456
                                                                0.0028397
                                                  66

-------
 RUN NUMBER

KAIEC(I)= COEF
            *  149 -G
                           5 10 VI
                 * U-Xin/72) * Y20?**.4)  « (Y02**.63)  *  WI20**.73)
     WHERE  CO£F=  .000159 * CXI' I 5520*{ 1 / ( T «460 ) ) )
             XS=    0.38000          T=  150.00000
   _  ..... „ YSQ2 = ._.- 0.00150. ________ YU2- ...... ..0..02QOO _____________________ . _
           YH20=    0.10000
._ XdJ.GMS- H2SO'i/.GH_C-  - - ..RAIE*-JGHS..H2SQ/1/.GH C-.M1H. . ..CALCULATED. .RATE .1. CHS H2S04/.CM .CrHIN _.
                                                                                               . Dif-ru i.
0.00569
.Q...OQ682 	 __. 	 _.
0.00796
0.00910
... .0.01023 	 	 	 _
0.01137
0.01421
0..01706- _ , .....
0.01990
0. 02274
. 0.0.''i59-.-. .. _ .. — _.
0.0?343
0.03127
0.03412- 	 	
0.03696
0.03980
0.04264 - — - - . -
0.04549
0. 04833
0.05117. 	
0.05402
0.05686
0 O6''i';
0.06823
0.07392
. 0.07960
0.08529
0.09098
. _ . _ _ 	 o# 09666 > • •
0. 1023i
0.10803
n 1 1 17?
0.12509
0.13646
0 14784- —
0,15921
0. 170U8
	 ft t Q 1 f> r:
0. 19332 - -I
0.204?0
0.01<>10UO
	 JO. 01 37051
0.012MOI
0.01-12231
	 	 J) . 0 1 0 1 9 73. 	
0.0092536
0.0071223
... - .0.0054766
0.00't,?3'i6
0.00.1'iH02
_..O.DO?.9137 	 _ .. .
0.0025U99
0.0021960
.. 	 Q. 00202 \'i
0.00190',!
0.0018211
. 	 0..00175&J
O.OOU131
0.0016781
_..- . O.OU16'(3Q
.0.0016106
0.00107S3 J
-U.UU1 •> 102 -_
0.0014569
0.0014029
0-.00l3'il6
0.001305.T
0.001251C
0.001197'J
0.0011439
0.00101J72
0.001^^79
0.000906'>
0.000787"
-0, 00067 7 I
0.0005774
0.0004856
0 .000404 7
0.0003345
0.0002779
0.0015665
	 „. 	 0.0015618
0.0015570
0.0015523
- _. . 0. 0015475
0.001542?
0.0015300
0.0015 189
0.0015071
0.0014952
	 	 _ _ 	 0. 0014833
0.0014714
0.0014595
0.0014476
0.0014357
0.0014238
0.0014L19
0.0014000
0.00l3fi0l
0.0013762
0.0013643
0.0013524
^ r* '« * T i i /
0.00130'iS
0.0012810
n.nni?S77
0.0012334
o.ooi2096 . :-;. •'•
n.oni i nsn .•••'*.'•
0.0011620
0.0011382
0.001 1144
0.0010668
0.0010192
' . , n.nnn^7i A . .
0.0009240
0.0008704
0.0000:'!19 . -
0.0007813
0.0007337
0 . 0 1 3 5 4 1 4
P . 0 K' ! '» 3 J
O.C1U05 !1
0.0096 708
o.oy >'t, '>()'<
0.00/7109
0.00';5915
0.0039*577
o.oo;.' rs.ub
0.lilH99
O.OU04685
0.0003973
0.0003444
0.000313;?
0.0002900
0.000/'66I<
0.0002463
O.OOD2259
o . o o n ' & 7 f.
0.0001.521
0.0001219
0.0000944
0.0000724
0.0000422 "
0.000012L
0.000018!
0.0000510
n.nnnciHAA
0.0001604
0.0002314
0.000,'>94S
0.0003467
0.0003908
O-OOO'.;1/,?
0.0004468
0.0004558
  MEAN  DEVIATION  «    0.0011285   R'JOf  MEAN  SQUARE DEVIATION
  RESIDUAL  SUM OF SOUARHS « 0.19Q76E-03
  MEAN  PEKCCNT DEVIATION = - 39.9634B57	_-,	:	 	
                                                                  0.0023497
                                                   67

-------
   RUN NUMBER =   150-G
5 11 71
        11= COCP  *  ll-X(l)/72l  « Y202»».4) *  (Y02**.63)
     WHKRE COEF-  .000159  *  CXP(5520*(I/(T*460)))
             XS--    0.30000          1=  150.00000
     .._. _--YS02-.--  0.00050	Y02=	0.020CO-.
           YII20--    0.10000
                                                          * (YH20**.73J
.. XII ),GMS H2S04/CK. C	RATE, ..CMS H2-SOWGK.C--.MIN	CALCULATF.O..RA.TE, .GHS H2S04./GM..C-HIN...
                                                                      OIFPtt)
0.00427
0. 00533
0.00640
0.0074V
_ 	 0.00853 	
0.00960
0.01067
_.. 	 	 0.01333 	
0.01600
0.01867
... . .. 0.02133
0.02400
0.02666
0.0793 A
0.03200
0.03'r66
- ... 0.03713 .. _
0.04000
0.04266
0.04533
0.04800
0.05066
Q f\r, i t •»
0.05866
0.06400
0.069J3
0.07466
0.07999
	 - -0.08533 	
0.09066
0.09599
- 0^40133
0.10666
0. 11733
- . 	 0.12799 	
0..13866
0.14932
0.15999
0^17066
0.18132 '
0.0162019
-O.Ol32?'iO
0.0112303
0.0095647
	 . 	 a.oo'a 15 i/i 	 : 	
0.0069400
0.0059054
	 0.0039369 	
0.0026751
0.0013675
. 	 0.0014637 	
0.001211 J
0.0011180
0.0010423
0.0010120
0.0009994
0.0009042
0.0009/92
0.0009691
0. onrioc.no
0.0009489
0.0009413 . '
	 0. "nno-
0.0009110
0.0008984
0.0008732
0.0008505 :.
0.0008303 /. ..: ;:-,
0.0008101 . . •••';'
0.0007849
0.0007621
C. 0007420
0.0007167
0.0006663 ;!
0. 0^06157
0.0005562
0.0004946
. - .0.0004109. 	
0.0003407
0.0002624
0.0010133
	 0.0010104
0.0010075
0.0010047
_:._ 	 _u 	 : 	 0 . 00100.1fl 	
0.0009VB9
0.0009960
	 0. 0009889 	
0.0009817
0.0009745
_ 	 	 	 	 0.0009673
0.0009601
0. 0009529
0.00094'J7
0.00093U5
0.0009313
0,0109241
0.0009169
0.0009097
. .,-0.0009026
0.0008954 :.
0.0008882 -
.... •_ • _ _ _.R.onnnnin . . •• :
0.0008666
0.0008522
Q. 000837ft
0.0008235 ..-•'., :
0.0008091 -:::<:.:>. i..
• '. . L. . n_onfi7Q^7 • ' ., ''•
0.0007803
• 0.0007659
O.OOO?'1!''
0.0007372
'"•-.'. ;,: 0.0007084
.rt,nnphjaf.
0.0006509
0.0006221
n, oOnr>.•:•••<
0.0000212 '*'$
n.nr)oniri'»
0..0000046
0.0000038
n.nnnnnqA
0.0000205 '.,
0.0000421 •.::;'
fi.finoo&39
0.0000956
0.0001275
n.nnoi ?/i4
0.0002239
0.0002734
 HFAN  OCVIAIION -   0.0003888    RUOT  MEAN SQUARE DEVIATION
 RtSlOUAL  SUM OF SOUARfS = 0.37030E-04
 MtAN  I'tRCtNT.DEVIATION.=- -20.6231304	,		_„,	...
                                      0.0010436
                                                  68

-------
RUN NUMBER =  151 -G
                             12 71
 RATECU) = COEF * tl-Xtn/721  * Y202**.'.)  *  IY02**.63) *  (YH20**.73)
    WHERE  COCT= .000159  *  EXP( 5520* ( I/ I T + ',60) I )
            XS=   0.38000          T= 300.00000
      ______ Y-S02 = -. 0.00250 _________ _Y(]2? ___ 0..020QQ ____________ _____ _  _  _________
          YH20=   0.10000                                           ...  ...... ~

_X1I ) ,GMS-H?S04/GM..C ---- IRATE, ...GHS..H2SO'i/CH..C-:MIN. __ CALCUI.ATED..RATI;,  CMS H2S04/.GM. C-N1 N.
                                                                                                IMFP.U )
0.0016*
..0..00327 ..._
0.00491
0. 00655
... . .0.00819 	 	
0.00982
0.01146
O.OI.HO
0.01473
0.01637
. 0..02046
0.02456
0.0286"*
0.0327'i . .
0.03684
0.04093
.0.04502 -
0.04912
0.05321
	 0.05730 	
0.06139
0.06549
0.0695U 	
0.07367
0.07777
0*08186
0.09005
0.09823
0. 10642 -
0. 11460
0.12279
0. 1309.8
0.13916
0.14735
0.0028032
	 — .. 	 JO. 0020756. . 	 , 	
0.0014617
0.0010903.
_. 	 	 	 0.000.9207. 	 	 	 _...
0.00000/6
0.0007268
	 	 ... 0.000666")
0.0006219
0.0005896
.. ... .. 	 0. 000*5330
O.OOOiiO't/
0.0004U45
__. 0..0004765
0.000*684
0.0004644 .
0.0004604 , ,
0.0004563
0.0004483
	 , 	 o . 00044 42_.™ 	 	 	
0.0004361
O.OU04200
ri_nnn/( i
O.OOO'il iv
0.0004078
J3. 0003957
0.0003796
0.0003635
0 .000147?
0.0003311
0.0003109
O.f>00?90l
0.0002665
0.0002463 .
0.0003256
0.0003242
0.0003228
0.0003214
	 	 	 .0.0003200
0.00031U6
0.0003172
0.0003L57
0.0003143
0.0003129
... . 	 	 0.0003094
0.00030'>9
0. 0003024
0.000?9Hrt
0.00029'j3
0.0002910
O.OOQ?fif'.l
0.0002847
0.0002812
	 ._, 	 0.000277V
0.0002742
0.0002707
D,000?67l
C • vwvt.o3£t
0.0002601
0.0002566
0.0002495
0.0002425
0,nno^'4S',
0.0002204
0.0002213
0.00021'. 3
0.0002073
0.0002002
0.0025576
0 .001 /S 1 'i
0.001 13H9
0.00076B9
	 	 .0. 0006007.
0.00040-n
0.000409/
0.000 3l»05
O.OOOJO/6
0.0002766
0.00022 U.
0.000190'.)
O.OOtH«22
0.000 I I'll
0 . 000 1731
0.0001726
0.0001721
0.0001715
0.0001670
	 0.0001665 	
0.0001620
0. 000l'i74
0.00011^6
n, non I A«'<
0.0001477
0.0001391
0.0001301
0.0001210
_ . .. Q..Q0011LU _
0.0001027
0.0000096
0.0000/65
O.OOU0593
0.0000461
 MfrAN DEVIATION =   0.0001712    RCOf MFAN SQUARE  OCVIAT10N
 RES10UAL SUM OF SQUARES *  0.10021E-05
-HtAN -PERCENT-HE VI AH ON-.-	36.7831726—-,,	,	_~
                                                                 0.0001892
                                                   69

-------
RUN NUMBER =  152-G
5 14  71
RATECU 1= COEF
MHERE COEM
XS =
YSQ? =
YH20 =
XII »,r,MS..H2S04/
0.00165
0.00331
0.00496
0.00661
. 	 . . 0.-00827..
0.00992
0. 01157
.0.01323
0.0l'i88
0.01651
0.02066
0.02480
0.02891
0.03J06
0.03/20
0.0'. 133
- 0,04546 -
0.04960
0.05373
	 -0.05786 -
0.06199
0.06613
0.07026
0.07439
0.07853
- - - 0*0 3266 -
0.09093
0.09919
0. 10746-*
0.11572
0.12399
	 0. 13226.
MEAN DEVIATION
RtSlOUAL. SUM OP
* (l-XID/72) * Y202*».4) * (Y02»*.63) * (YH2U**.73I
.000159 * EXP(5520*( 1/IT+460II J
0.38000 1= 300.00000
n.nnisn Yn? = o.o?noo
0.10000
CM C. RATEf CMS H2SO'}62
0.000'iOlB
0.0003902
	 0.000 W,67 	 _..
0.000.1 '.72
0.00032/7
0.000 HI ^1
O.OOOiOU'i
0.0002S8V
. n.non?v*i
0. 000261'.
0.0002536
	 O-0002/i 5.7 	 : 	 	
0.0002380
0.0002302
n oor'JZ?'-
0.0002185
0.0002107
	 .,. 0.0002028
0.0001951
0.0001872 :- -
.'..-'..'.'.. 	 . P, 00" 1795- : .
0.0001717
0.0001599
0.0n0lr'22
0.0000539 ROOT MEAN SQUARE
SQUARtS-S- 0. 17.109L-06 - ._
	 CALCULATED. RAT E ... GHS .H2SU4/GfL£rHI N 	
0.0002654
0.0002643
0.0002631
0.0002619
O.OOOP60B
0.0002596
0.0002585
0.0002573
0.0002561
0.0002550
	 .....-„ 	 	 0.0002521 .. 	 	 	 ...
0.0002492
0.0002463
0.0002434
0.0002405
0.0002376
(l.000,'347
0.0002318
0.00022B9
	 	 „_ 	 0.0002260_ 	
0.0002231
0.0002202
•• • . • ii-onu./i Y <
0.0002144
0.0002115
0-00020RA
0.0002028 .. . .
, '••: . 0.0001970 " '"."•
••'•"•' o.oooi^i y '• •
0*0001854
0.0001796
, , , n.nnn)7^f«
DEVIATION = 0.00008H "-;vv • ;
— 	 O.lPF(.l) ._
0.0004680
.O.OOOJ444
0.0002987 	
0.0002453
0.000215?
0.0001929
0.0001707
0.0002389
0.0001457
0.0001352
0.0001146
0.0000900
0. OOD0015
. .0.000060 /
o.oooo'j';9
0.0000511
0.0000384
0.0000296
0.0000247
.0.0000198 	
0.0000149
0.0000100
U •. WU U U ti j*J.
0.0000041
0.000000-8
0^0000057
0.0000077
0.0000098
n.nnnoi \ 7
0.0000137
0.0000197
0. 00002. Ui

                                            70

-------
 RUM NUMBER =  153-G

RATEC(D=  COF.F
                          5  18  71
               * (l-XIM/72)  * Y202*».4)  *  (Y02*».63) * tYH20**.73)
   WHERt  COtF = .000159 *  FXP(5520*(t/ ,
0.07349
0.07961
0Tnnr,74
0.09186
0.09798
0» ln'»l I
0.11023
0.11636
0. 12240
0.13473
0. 14698
0. \*o??
0.17147
0.18372
	 . . 0. 19597 	 ,_.-
0.20822
0.22046 •
	 ... 0T?^?7i
0.24496
0.25721
	 	 . 0. 26946
0.28170
0.29395
	 -.-0.30620 	 	
0.31845
0.33070
- 	 O.J429',
MEAN DEVIATION = 0.0007441
-HE SI DUAL- SUK-J)r.-_SCUARES-K~.0»
MtAN PERCENT DEVIATION = 39
0.0178058
._ 0.0159658 	
0.0141259
0. 0125234
0.0109802 _
0.0096151
0.006V068
.0.0043921
0.0034128
0.002V599
.0.0024-..72 .._. 	 i 	
0.0022S14
0.0020654
.....0.0020120 	 . . ,
O.U019646
0.0019230
.. ..Q .00 1 Wt'i 	 ,.: 	
0.0018518
0.0018191
	 Q .00 1 7.924 	 	
0.0017628
0.001/3'JO
_.o.noi/,9/s
0.0016559
0.0016144
O.noi r>72fl
0.0015254
0.0014838
n,Ofi)/>TA'4
0.0013829
0.0013355
n.nn) ?R79
0.0011811
0.0010802
0.00097"*
0.0008665
0.0007538
-0.0006'tlO. 	 	 	 —
0.0005401
0.0004570
0.0003799.. , . . 	 	
0.0003264
0.0002849
0.000249 5
0.0002255
0.0002077
_,.0. 0001899. 	 	 	 	 	
0.0001662
0.0001543
_0. 0001424 • 	
ROOT MEAN SQUARE DEVIATION
1 7 7 A-H r- - fi 1
.2494659
0.001919',
	 Q.0019UI 	
0.0019069
0.0019006
0.001H943
0.0018880
0.00187i!.l
0.0018566
0.001840U
0.00 182 5 I
	 0.,00180'K,
Q.0l>ll'i.\r
0.001 7700
0.00] «>22
0.001 /465
0.0017308
	 0.0.017151 	
0.0016994
0.0016836
_— ..0...00 1667-9. 	 , 	
0.0016522
0.0016365
0.001605.0
O.OOl5Mt>
0.0015422
0.0015107
0.0014793 -.•••:
0.0014478 V
	 0.0014164 :
0.0013850
0.0013535
o.onj3P?i
0.0012592
0.0011963
0,001 1H4 ^
0.0010706
0.0010077
	 0.00094. 40
0.0000019
0.0008190
... _. 0.0007562. 	 	
0.000693 1
0.000630't
	 0.0005675 . . ._
0.0005046
0.00044 18
	 	 0.0003789 	
0 0003160
0.0002531
0-000190?
0.0019649

0.015HU63
	 ... .0.0140527
0.0122191
0.0106^2!)
0 . 0 0 V 0 8 S 9
0.00/72/1
0.0048345
0.0025355
0.0015/19
0.000934U
0.00064 /«
0.0004'j 1 1
0.0002H75
0.00'J/"f9(i
0.0002U<1
0.0001 922
	 	 O.OOOU.93
0.0001524
0.0001355
	 	 .__.0. 0001245. ....
0.0001106
0.0001026
O.OOOU9/5
u.OOoOoi j
0.0000723
0.0000621
0.0000461
0.0000360
O.OOD0199
0.0000020
o.ooooini
0.00003',)
0.0000/81
0.0001)6!
...0. .000 1600..
0.0002040
0.0002539
0.000303U...
0.0003418
0.00016?0
0.0003/63
O.OOO'J/,69
O.OU03455
0.000311)2 .
0.0002 I'll
0.0002140
	 . O.OOOIU90
0.0001498
0. 0000988
0.00004/fl ...


                                                     71

-------
 RUN MIUBER «  157 -G
5 31 71
RATECIl)= COEF * Il-XIM/72) * Y202**.4> * (Y02**.63t *  (YH20**.73>
   WHERE COEF = .000159 * EXP15520 *(I/IT4460)))
           XS=   0.30000         1= 200.00000
         _YSQ2=.	0.00200	Y02j=
YH20= 0.15000
.XII) .CMS .H2SQ4/GH..C 	 RATE., _GMS .H2S.Q.'u'GK_C-J-UN 	 CALCULArEO_flAJ£.«__GMS .H2SOV..GM .C-MLN. 	 Plf.F.U )
0.00272 0.0052234 0.0012000 0.0040234
0.00407 0.0039256 0.0011956 O.OOPMnn
0.00543
0.00679
	 0.00815
0.00951
0.01087
	 O.OJ222.
0.01350
0.01698
0.02037
0.02377
0.02716
0.03056
0.03395
0.03735
0.04075
0.04414
0.04754
0.05433
0.05772
	 0 • Oo i-1 £• -
0.06451
0.06791
-. 0.07474)
0.08149
0.08828
0.09r>07
0. 1U186
0.10866
0. 11145
0. 12224
0,12903
- 	 - .0. 13582—
0. 14940
0.16298
-0. 17657 -
0. 19015
0.20373
0.21731
MCAN Of VI AT ION
RESIDUAL SUM OF
0.0025J06
0.0014275
n.OOlPOl? 	
0.0012328
0.0011939
	 	 	 0.0011615 	 _„_
0.0011420
0.001 1096
0.001 lO'll
0.0010966
0.0010901
. . . . 	 -.-0.0010771 	 	 , .
0.0010706
0.0010576
_ 0.0010447
0.0010382
0.0010317
0.0010122
0.0009992
O.OOOV/98
0.0009668
0.000q408
0.0009149 ..:.; '•:•-.
0.0008089 : :
	 ... 0.1008630, ''";••
0.0008371
0.0008110
O.Qnn7A';j
0.0007592
0.0007397
0.0006878
0.0006489
0.0005516
0.0004996
__•-• _ 	 0.0004477
« 0.0000383 ROOT MEAN SQUARE
SQUARES..* 0.57829E-07 	
0.0011913
0.0011870
_. _. 	 	 0.0011827
0.0011784
O.OOU740
	 0.0011697 .
0.001 1654
0.0011546
* ' 0.0011430
0.0011330
0.0011222
	 	 I... 0.0011114 .. .
0.0011006
0.0010R98
0.0010790
0.0010682
0.0010574
0.001046'!
0.0010358
0.0010250
.... ._ 	 _.0.»001DL42
0.0010034
0.0009926
''.:••;• . 0.0009494
', ' 0.0009278
0.0008846
0.0008630
0.0008198
0.0007982
0.0007334
0.0006902
0.0006038
0.0005606
n,0i)0r>174
DEVtATlON -- 0.0000406
0.0013393
0.0002405
0.00010H6
0.0000545
0.0000199
	 	 	 ...0,0000083....
O.OOU0234
0.0000450
0,000040?
O.OOOU3C.4
0.0000:121
	 	 0.0000343 	
0.0000300
0.0000322
0.0000344
0.0000300
0.0000257
0.0000?79
.: . ..:. 0.00002.36
•- ' ' ' 0.0000258 ;
0.0000258
n.onnfMn?
.•" ' ' 0.0000345 .;•
..; 0.0000309' ,
0.0000476
0.0000520
0.0000563
O.OOU0607
O.OOU0586
n. 0000564
0.0000456
0.0000414
0.0000436
0.0000523
0.0000610
Q.000069/

                                                  72

-------
  RUN
      NUMBER =  158 -G
I 71
 RATECIII-  COEF * fl-Xtl)/72) * Y202»*.4)  * (Y02**.63> *  (YH2D** .73)
    WHERE COEF- .000159 * EXP'( 5020* ( I/ ( T K60) ))
            XS=   0.38000          1-  300.00000
    	YSD2«	0..00050	.	Y02=_	0.0.2000		     _	
          YM20=   0.10000                           ~            '            "  "    	~	"

., XU).GMS..H2S04/GM C	-RATE ,..CMS_ H2S0.4/GK .C-K1U. ...CALCIILAT tl)  RATE,..CMS H2S04/GM_C-MIN	  OIFF(| )...
0.00155
O.OOJ1Q 	 .. ...
0.00466
0.00621
. 0..00776 	 , 	
0.00931
0.0108/
O.m2.42 ., 	
0.01307
0.01552
O.XH9'iQ 	 _..
0.02329
0.02717
... J)..031Q5 	 _ „_. ..
0.03<,93
0.03881
	 0.0'>'.>
o.ooo 16 '.a
0.0001630
0.0001613
0.0001595
0.0001577
0.0001560
0.00015'.2
0.000.15 25
0.0001507
0.0001't90
	 0.0001472..
0.0001455
0.0001437
0. 0001420
0.0001402
d.ooonu'i
	 .0.0001367..
0.0001332
0.0001297
0. 0001^6?
0.0001227
0.0001192
0.0001156
0.0001121
0.0001006
_.. .IK 000.10 5. 1..
O.OOOJ6B8
O.OOl.ViH'i
O.OOOl'J/9
0.0001 /OS
O.OuOl',97
0.0001320
0.0001 171
0.0001038
0.0000926
0.0000315
0.0000603
0.0000'.36
O.OOC029a
0.0003.153
0.0003224
0.0000026
0.0000038
0.000009!*
0.0000144
	 0.0000178 	
0.0000212
0.0000239
0.0000258
0.0000278
0.0000297
0. 000031 7_._
0.0000341
0.0000372
O.OOOOHB9
0.0000405
0.0000422
0.0000431 	
0.0000441
0.0000451
__ 	 	 . . Q...OOOQ46Q. ...
 MEAN DEVIATION =   0.0000609    ROUT  MEAN SQUARE DEVIATION
 RES I DUAL-SUM OF-SOUARES_»-.a»28291E-06	
 MEAN PERCENT DEVIATION =   17.356/352
                                                                 0.0000988
                                                   73

-------
  RUN NUMBER =   160 -G
                          6   9  71
 RATECU) = COEF  *  (l-Xlll/72)  *  Y202*».4)  *  (YU2**.63)  * (YH20**.73J
    WHbRi; COCF=  .0001-59  *  EXP I 5520* (I/ ( T *460 ) i )
            XS=    0.38000          T* '200.00000
         _YSf)2 =	Q. 007.00	Y02=	0.02000	
YH20 =
XI 1 1 iGMS..t!2S04
0.00322
0 ..004 11 J
0.006'. 3
0.00804
0-00965
0.01126
0.01287
	 0.01448
0.01608
0. 020 10
0.02413
0.023 1 '.>
0.03217
0.03619
0.04021
0.04423
0.0482'j
0.05227
0.05629
JO, 06031
0.06434
0.06836
0.07640
0.08042
0. OH846
0.09650
0.10455
. . - .. O.-l 1259
0.12063
0.12867
0.05000
/GM C 	 RA.I.E,..GMS_li2.S04/G.H
0.0030573
n.nn?| si?
0.0015207
0.0011031
0.0009377. ..
0.0000274
0.0007328
	 	 	 0.0006697... ..
0.0006146
0.0005358
.-...:., 	 	 .._ . .0.000.5043 	
0.0004806
0.0004728
_ . . _ 	 	 _ 0.0004570 	
0.0004491
0.0004334
0.00r>
0.0004176
0.0004097
0.0004nio
0.0003861
0.0003782
0.0003703
0.0003625
0.0003546
0.0003467
0.0003388
0.0003.309
0.0003309
CL-MUL. CALCULA.T.EO_RATE, .CMS ..H2SOWCM C.-JU.N
0.0005374
0.0005351
0.0005320
0.0005303
0.0005259
0.0005236
_ 	 	 	 	 0.0005? 1.3 	 	
0.0005190
0.0005133
	 . 	 : ._ 	 	 0.00050/6 	 	 	
0.0005018
0.0004961
	 .„._. _ 	 ,.. _.„ _ 0.0004 904 .. . . . •
0.0004U46
0.0004709
'.;. 0. 000473?
0.0004674
0.0004617
0.0004502
• .-• ; ; o. 0004445. :
O.OOC'.33Q
0.0004273
: . : ••;. • • 0.0004043 :. ..•
;';?."•". '-''. •': '•' 0.0003929 ,;; •'•/; \", .
0.0003699
0.0003585
OIFF(t )
0.0025199
0.0016161
0.0009879
0.0005726
0.0004095
0.0003014
0.0002092
0.0001484..
0.0000956
0.0000225
.... 0.0000033
0.0000133
0.0000233
0.0000333
0.0000355
0.0000455
0.0000477
0.0000498
0.0000520
fl. 000054 L
0.0000641
0.0000663
n. 0000627
0.000064S
0.0000612
0.0000577 •
0.0000541
0.0000465
0.0000390
0.0000275
 MtAN DEVIATION -   0.0000670   ROOT MEAN SQUARE DEVIATION
 RfcSIOUAL SUM OF SQUARES = O.?1707!l-06
• MEAN PERCEfJl-DEVlAflON =—13,8535900—	
                                                                0.000091't
                                                  74

-------
RUN NUnilPK =   161 -(!
                         6 10 71
RATECI 1 1- COC-r
WHCKC coor-
xs-
YSU2--
YH20-
X(l ) .CMS .H2';(>4/
0.00292
0.00'. 30
o.oor.H'i
0.00/10
o.o on/ 6
0.01022
O.OIU.H
0.0131 r>
0.01461
0 . 0 1 U 2 6
0.02191
0.02V./.
0.02921.
O.OJja/i
0.03651
O.O'iOl /
.. ..0. U43H2
0.04/47
0.051U
	 0.0547 7
0.051142
0.0620«
0 n A '» r *
0.06930
0.07303
. . .. 0.0003.3
•0.08764
0.09494
0. 10224
0. 109',4
0. 1 I(,!I5
0 . I 2 •'* 1 .5 .
0. 1 1145
0. 138/6
0. 14606
0. 1606 /
0 . 1 / 5 2 /
- 0.189'ia
Ml. AN IKVI AI KIN
Rl 3) * (YH2U**.7.3I
.000159 * tXIM 5520« I I/I 1*4601 1 i
0.30000 1= 200.00000
.. 0.00200 . 	 YU2- ,.0.02.000
0. 10000
•T,;i c. RA.rr, C.MS M;-Mi4/r,n C-MIN CALCULATCU
0.00'.. 97 14
0.0042(17 / 	 	
0.0030/114
0.00] 9/90
O.OO.l.'46U 	 	 _
0.0010481
0. 0009455
0.000(1/22
O.OUIKI429
0.000 flu/. 3
0.000/H'i 1 , 	
o. (10 o//,.-: .1
0.000 /',49
0.0007402 	 _
0.000/25/,
0.000 7 U12
	 0.000/03.',
0.0006963
0.0006963
	 0.0006^90 ....' 	 _. 	 	 	
0.0006P.90
O.OOU6JH 7
11. llt'll'W.M 1 i
0.0006/43
0.0006670
	 	 _. . o.0006T,9/ . 	 	
0.0006523
0.0006W6
	 	 	 •. 	 0.0006210 	 	 	 	 _.
0.00061-1.'.
0.0006010
O.OOOMI64 _ _ .
0.001)571 /
0.000','. /O
0. nnO', 35:1 	 	
0.0004.91 1
0.0004471
0.1)00 J'j'.iO ... - 	
0.0000', 61 ROOT M1:AN SQUARE OEVIATIIIN '
^i IIAUI ( .. n. i I'l'ioi -n/>




RAIT, CHS II2S04/GM C-ttIN
0.00011920
O.OOOBf.ifl6
O.OOOHUM
0.0008UI/
0.00007U2
0.0000/43
O.UOOU/1 3
0.00006/9
0,0000644
0.000li')',«
0.0008471. _ 	 	
0.0000.3115
0.0000299
O.OOOU212
O.OOOH126
0.0008019
0.0007V5 i
0.000/867
0.0007780
..0.0007694 	 	 	
0.0007607
0. 0007521
ri 90<"i '4 TS
O.OOOTVio
0. 0007262
. 0.000/009. 	 	 	 	
0.0006916-
0.0006/44
. 0. 0006571.
0.0006398
0.0006225
0.000605.3 	
O.OOO'.KiaO
0.0005 /o;
0.0005514
0.0005109
0.0004843
0.000449R
0.0000651




OlIIMl)
0. 0050014
0.00 13991
0.002 19.12
0.00109/3
. .0.000 36 / 1
0.0001 / 14
0.0000 ,'42
0.000004 1
0.0000215
0.000049!.
0.0000629
0.0000/62
0.0000/49
o.oooofJin..
0.00001169
0.00001357
0,000091 /
0.0000904
o.ooooaio
. 0.0000404. ...
0.0000718
0.0000704
. 0.0000618. ..
0.0000'-05
0.0000592
0.0000492
0.0000193
0.0000 J6/
. 0.000.0:i4 1
0.0000242
0.00002] 5
O.OOUOU1.9 . .
0.000016 i
0.001,0117
0.00001 1)4
0.00002 /(I
0.00001/2
O.OU00539

                                                 75

-------
KUII NUMHP.R -  162-G
6 11 71
RACC-Cltr- COCF * (l-XtI)/72)
Wllf.KE Cl)EF= .000159 * HXPI
XS= 0.38000
.. .. . .YS02= .0.00200 	
YH20 = 0.10000
XI I ) .GMS-M2S04/CH C- _.RATE-..-
0.00149
.. .. 0.00298 - 	 	
0.00448
0.00597
0.00746
0. 0009'j
0.01044
0.01193 .. . .. . . 	 	
0. 01343
0.01492
0.0186S
0.02238
0.02611
0.02934
0.03)57
0.03779
0.04475 	 ..-. ...
0.05221
0.0596/
	 O. 06 Z 13 	 	
0.07459
0.08205
0.09697
0. 10443
0.11180 ,....___.
0.11934
0. 12680
0* 13426
0. 14172
0. 14918
0. 16410
0. 17902
0. 19395
0.. 20085 	 .... -
0.22377
0123869
- . ... 0.25361 . . . „ .. 	 - -
0.26852 ,
0.28344 '
- 	 0.29836 . - 	 -
0.31328
0.32820
WAN DEVIATION = 0.0010756
Rl MODAL SUM OF SCIIARt-S » 0.4
-MEAN PERCCM DC VI AT J ON . -._ 63.
* Y202**.4)
T= 200.
....Y02--.. 0.
* (Y02«*.63) * (YH20**.73I
460) ) I
00000
(17000
.CMS .H2SCK/GM..C--HIN 	 CALCULATED. .RAT.E, CHS
0.0069869 0.0008954
0.0050647 - .0.0008919
0.0046338
0.0030410
0.0017667.
0.0015929
0.0015639
0.0015.71)4..
0.0016146
0.0016436
0.001 7304
0.0016028
0.001116(10
0.00) 9107
0.0020200
0.002092'i .
0.0021576
0.00220 1 1
0.0022300...
0.0022517
0.0022517
'* ^ C *I 2 ** "Z **
0.0022155
0.0021938
.0.0071504
0.0021142
0.0020708
. 0.-007073-3-
0.0019766
0.0019107
,. 0.001.7956.™
0.0016653
0.0015204
O.UQ13/V/ .
0.0012309
0.0010716
-0.0009051-
0.0007675
0.0006444
.0.000r>3'i8
0.0004344
0.0003692
HOOT MF.AN
0115 lt-04
B6044J1 	
O.OOOU884
0.0008 8 '.»
0.0008(113
0.0008778
0.0008743
	 _._ 	 	 	 	 	 	 0.0008707
0.00006/2
0.000(1637
0.0008548
0.0008460
0.00083/2
. ., . ... 0.00002(14
0.0008196
O.OOOU107
.. _ . _ _ 	 _. ...0.0007931
0.0007754
0.00075/8
. . .„' 	 , 	 	 	 	 	 	 0.0007401.
0.000722S
0.0007049
0.0006877
0.0006696
0.0006519
0.0006343
. . 0.0006166
0.0005990
0.0005637
0.0005460
0^0005 108
0.0004755
0.0004402
0.0004049
0.0003696
0.0003343
	 	 _.. 	 	 0.0007.990
0.0002637
: 0.0002 2 04
0.0001931
0.00015/8
0.0001226
SQUARE DEVIATION = 0.0011491

K2S04/GH_C-.mN 	 OIFIMI)
0.0060915
0.0037455 	
0.0021561
o • o o o u y 5 '(
0.0007151
0.0006897
	 _ 	 0.0007077
0.000/474
0.0007799
.. 	 .. 	 	 0.0000756
0.0009568
0.0010300
	 0.0010903
0. GUI 1491)
O.OOI7.U9 1
0.00l79')'i
0.00131)22
0.0014433
	 „ 	 	 	 0 . 00 1 4 89r; 	
0.0015292
0.0015409
	 	 O.OQ1.55.0Q..... .
0. 0015460
0.0015419
O.Ofll "5161
'.;•' 0.0014976
. ;'..::.. 0.0014718
0.0014129
0.0013/26
0.0012849
O.OOU898
0.001O003
	 ___ 	 	 0.0009708 _..
0.0008613
0.000/3/3
,.. 	 , 	 .. . . 0.0006061 ...
0.0005037
0.0004160
.. . 	 	 	 	 	 0.000'Vt?6
0.0007766
0.0002467

                                               76

-------
 RUN NUMBER  -   163-G
6 1'. 71
RATtC47) „, .-. .- 	
0.0004953
0.0004 4 U.

.RA.Tl:i._GMS..II2S
0.0008851.
0.00080)6
0.0008 lu I
0.0008/47
0.00.08712 	
0. 000867 '/
0.0008643
O.OOOB556
0.0008409
0.000(1 'Jit 2
0.0008296
0.000820'y
0.000111 22
0.00080 )'..
0.0007949
0.000/062
0.0007775 . ....
0.00076CO
0.0007602
O 0 ') O 7 f\ 1 5
0. 000/428
0.0007342
...0.0007255 	 . _.„ 	 	
0.0007001
0.0006908
O . OO06 73 4
0.0006561
0.0006387
ft - OOQ6 21'.
0.0006040
0.000506/
. 0.0005644.. .. __ 	 .
0.0005520
0.0005173
.. 0.0004826 	 	
0.0004479
0.00041.32

	 	 uif-r ( i )
0.0021580
0.0016210 	
0.00 I 1 595
0.0007V 85
O.OOOV162
0.0003788
0.0003083
0.000 2 527
O.OOU2044
0.000 I ft}')
o.oooiov;
o.oooo 1 1 1
o.oooo n 2
0. IM.l'll) !.>;<
0. OIH)l)(i.'> i
O.UOII06 Id
0.0000/26
O.OlKU) / 76
0.0000325
0.00110875 ,
O.OOC08L8
0.0000901
0 » 0000'* L 4

0.0000976
... 0.0000952 	
0.00009/8
0.0001003
0.001)0955 .
0.0000980
0.0000932
O.OOOQ95B
O.OOC0910
0.0000935
.. ..O.DOOOB87 ..
0.0000(130
0.0000742
0.0000'.'. 5 . ...
0.00004 74
0.0000304
 HI Al-j  1)1 VI ANON -   0.0001008    UllllI Ml_Afj
 RIS1UUAI  SUM 01' SoUAKfj - 0.44449J-06
 MIAN  I'iKCi.Nr UI.VIAIION  .  12.0020390  .
                                           '.UUAIU.  ULV1 Al ION
                                                                 0.0001143
                                                   77

-------
ItllN  MJKIU'i
                           6 15 /I
RATtU 1 1= C'lCr- * (1-XII 1/72)
MiCRE COI r- .000159 » CXC
XS= 0.3POOO
.. . . _ .YS02- . 0.00100 .. .
YH2G = 0.10000
Xlll.GMS ll2SO'i/G."! C .. RATlir
0.00146
0.0029?
0.00439
0.00505
0.00711 	
O.OOH7 1
0.01023
0.01 1 10
0.01316
0.01462
0 . 0 1 II ,' I
0.0?1''3
0.02',1, a
o.-'.r.
- 	 0.0621 i ... — 	
0.06579
0.06944
.... 0.0/310 	 — ._
0.0004!
0 . 0 II 7 7 2
0.09503 	 	 • 	
0.102.34
0. 10965
-0.1 1696. 	 	 .. - 	 -
0.12427
0 . 1 3 1 5 1)
O.IJBII'J ... .
0.14620
0. 160fi?
0. 1/544
M.M DrviAIlllN 0.00001.?!!
I'l. Ml.HIAl SUM HI SOUAKI. !> . 0.
<• Y202'> •:•.'.)
(5520*1 )/(T,
T= 200.
. Y02 = .. .0.

IK: ;;rs:;wG
0.0018122
0.0012529
0.000012-)
0.00070)35
. . 0.0006570 .
0. 0006 190
0.000604 t
0.00051)-.,;'
0.0005/4 »
O.OOO'.C.i,!!
0.0005',4'i
0. 0005. U,'»
0. 000 V ? 20
0 .OOOM'ift
0.0005U/1
O.OHO50 l'i
0.00050 J4
0.0004'; 76
0. 0004096
., O.OQO'.')')6
0.000'i'iOC,
0, rinn'.«M/,
.. 0.0004-J96.
0.0004996
0.0004996
0.0004996
0.0004922
0.00048'r7
0 0 0 0 't f * ^ 7
0.00047 73
0. 0004690
• 0.0004661 -

0.0004549
0.000'<4 /',
0.0004 V3
0.0004 176
O.OU03953
KHlll h| AN
1 /069I -06
* (Y02**.63) * (YH20**.73)
460) ))
00000
02000.. 	 	 .... . 	 	 	 	 	 .

M C-M1K .....CALCULATED. RA.T.Ei CHS 11250',/GH .C-'ilN 	
0.0006707
	 	 	 0.0006760 .......
0.0006734
0.0006703
... ... 	 .... . .. ..... 0.0006602
0.0006656
0.00066?-;
	 _ ..... 0.000660J
0.0006'. / /
0.00065-51
_ 	 U.00064U1;
0. OUU64 20
O.OOiK* '54
0. 0006 21! 7
0.000622 i
0. 00061',,!
... . 	 	 	 	 0.0006092
0.0006026
0.0005961
	 0.0005095
0.0005)) 30
0.000576',
	 	 ._ . 	 (j.ouuu.'iv-; ... 	
0.00056:* (
O.OOOli'JMl
0.0005502
0.000-53/1
0.0005240
-0.0005 109
0.0004970
0.0004047
	 	 	 , 	 	 	 	 0.0004/16 _
0.. 0004 5 85
0.00044'.',
	 . . 0.0004 323 	 	
0.0004192
0.000.5930
	 	 	 0. 000.5667 	
.".OUARl OPVIA110H >• 0.00007JO






	 .01 PC II )
0.001 1316
0.0005 761)
0.000 1 V;5
0.00003/7
0.00001 12.
0.0000465
0.00005UH
0.000071 I
0.00001)34
0. 000008 J
O.OUOlO'il
0. 0001050
0.0001 1 Vi
0 . 0 0 0 11 4 3
0.0001 15?
0.000 I 124
0. 00010511
0.0001030
O.OOU0965
0.0000099
O.OOOCKU4
0.0000768
0.00007^?
0.00006 ji
0.0000571
0.0000506.. 	
0.0000449
0.0000393
0.0000?62_
0.0000205
0. 0000149
0.0000055 .....
0.0000039
0.0000095
O.OOOOJ52
O.OOD013',
0.0000247
0.00002RI5. .


                                                     78

-------
                     APPENDIX A-4






S02 SORPTION RATE STUDIES IN 1 INCH DIAMETER FIXED BED
                          79

-------
                                      llAll
                                                            2 7)
   Tl I'l'l iiAK'RE  •   200,->0r>''<0  T
   tl-A'l  VI LOCI 11 ••     O.M'iTlll.  0'<  /MR
   HIM T •,'.);> ''oi r n>Aci )(•*<  (ti'Yi  •     Ct00?uoc
   lldll l(!0 full  ri'A-.TIO'i  »     0.059?i:7
   IHLI.T OXYGI-N  '-'Glf fl'/'llON  "     0«037I.:-3
   INI FT C02 M':,.r HUCTIJ.l  -     O.Of.OOOO
   IMl'T NO HO! F.  niACTH.M «     0,000000
   IH'-ll lilCFiT  6,\S HMC  FRACTION  -  .   0.900S63
   IMI:T CARBON  ULICIJT  •    >:.,nooooi  GMS
   T01AL GAS CLOW »     S.32991;'*  SO!H
                                                           (WET)
TIMI:

0.
20.
40.
60.
CO.
100.
120.
no.
no.
ieo.
200.
220.
240.
26P.
2BO.
300.
320.
340.
360.
ERACC
HOLF

0.
0.
0.
0.
0.
0.
0.
0.
• o.
0.
0.
0.
0.
0.
0.
0.
p.
0.
0.
RATE Of
FRACTION S02

OOOOUOE
'.•COCuC ..
420000L
4700001.
46000GE
560000F

00
J$
-03
-03
-03
-03
7'iOPOOl-03
910POC'!.
lOBCPilC
i ? 5 po or
140POO!
1560i Ot
1 70000!
10200PE
1940001
206POOI
216P001
2?iOPOI
?32000t
•-CJ
-02
-02
-02
-C?
-Ot!
-02
-02
-02
-02
-07
-P.!
S02 SOtPTJON •
H2'.,
GUS
0.
0.
0.
04 LOADING RATC 0
ACID/'.-
OOOOOOC
1", 33 1 0 E-
677?2!>l
o . i oo v ; o i.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
1 3 i A 7 6 E
16M05E
19<>':<.4E
22?.'P8t:
?',7317C
?69970t
?90'-07C
30569ft
3 ? 4 9 Ci V f;
3^V> ] 6i;
35S063F
3631'. 7t.
372 ? 0 7 1!
3BI02/I.
366JP5E
^\ C
00
-01
-01
00
00
00
00
00
00
00
00
00
00
00
00
00
00
HO
00
G^b
0
0
0
o
0
o
0
o
0
0
o
0
0
o
0
0
0
0
0
! II2SO.V SO-?'
/.CID/OM e -I
.OOOOOCif 00
i 1593 ^6f_-02
„ 1&4£!70!--1'<:
. lfc**C78t-02
* X6^' 107E- or
. UL 17*11-02
, l',2709f-OS
.1309-*2E-Ol:
. H9i^rf.-o/
, 107-J /fif-0?
. 9 6 9 £ ? .'? r - 0 3
,8i903r! -03
. 7620'! ?': -d )
*t7t!910r-03
. '.' 9 f> 7 7 V 1 - 0 3
.5126'.vr-03
.4',3370C-03
,387'?'.9r-03
.3J2L.27L-03
1033V6C-02
   AVI RACE K/il T or  .VoflCTluv HP

   TO H LoADi/vg cp  Ji,V  C<«5/icilj/ftt C
              CAS
                     SO? SOUPI IUM  RAff
                                                      3   8
 S"A(T  VI I 0(1 TV  -     r.r>
 INLI  I  ST."1 V;M.I  f ^ACI 10\
 IMf  1  -VC "01  '  rr,ATT |(r,

        CO?  '-'C.l  f  I r.'ACT ION

        I'.I'M GAS  VOL
 IM.I  T  cA'-<"()\  «ricni •    4i.'ocoon
 T'-TAL  f-A.S  H.:i\!      ],, .i.'QPO  f.CfH
                                f  0'.  /n'<
                                l  -     0.002701)
                                 O.OdlC89
                                    0.03'.710
                                 0,0000JO
                                C.000000
                                '< -     0.90746'.
   T I •->(
.•.l'!9.-.:.r
               1 !  f rac 1 1C',  ',('?
                                       XS ACIU/('" C
                                                        RATE Or  H?sn>.  -iOI'PTION
                                                           0VS  AC ID/ d1'. C-VIN
0.
70.
'.C .
63.
PC.
IOC.
!?( .
1 '• " .
!6C.
1 a ^.
™r .
7.T.
?<•' •
n-r.
o.c"r •:':)(
o.i!. •:-•:. rr
0 . 1 d .. '. 00!
0. 1 •;
0,
c.
0.
0.
0.
a
^
j
o
t.

tj? -\
'it,'.
»'><>
•Jf.B
•• v Oii!<. ;n
-'"f
-'..'
- 1! ;-
-12
- ;.'
-(.V
-[.?
-0?
:>.
o.
0.
0.
0.
0.
*'•
0.
<.
;
1
;

l
1
:
i' '7
1 )'.
,'J1
<)l
43r)
07 '
dli
69'.'
O'll
'- 7f
7')l
.6!
'/'
'VI
i; '. I
O')l
?fcl
ortt
(j.*C
;'.7t
(.sr
2CE
i<0
- C 1
-01
-01
-•01
-01
-ill
pa
00
:>u
JO
00
00
00
0
Q
3
D
2
0
0
0
0
0
3
0
3
o
,0'jooru''
*.96ft / ' [
. H,i,2 ).'!
. l',3is\
. i'j'ni.',(

.(-6 JO'. )f
.'•Oll'd 71
«'j'j'. 7V1I
.OJ/'. ! 11
.'• '36 ';,' -"
.i.397 Ml
• 426? -i j^
.^>19'i76l
00
—03
-03

-03

-0..
-01
-O.I
-03
-0 3
-03
-03
-•03
               or ;,r-j
1«  A  LofitifCt ''/  /.Vf
                             ION •     OO9907Bt-03
                            uf

                             A I )>/(./•/ C  =0. OS'/L-

                              =   /.CO   f)/M-(
                                                                          c  --A/Ay
                                        80

-------
                   S02
                                RATE
                                                 3  '.75
SA-5

TEMPEPATUtU  «   2CO.OOOCSO F
SPACE VCLOCI'il  •     O.fc0?3£.7l. 0"ACTION -    0»CJ9f.9o
INLET OXYGEN' k'-nir FRACTION "    0.0j~032
INLFT CO?  HOI.i  FRACTION •=    OtOOOOOO
INLET NO MOLL  FRACTION  •    O.UOOOOC
INLET 1*1 ra  GAS HOLE Ff;ACTICf. "•     0.9039?:)
INLFT CA'':"'Vi WCIGHT »   ICiiAOOJO QMS
TOTAL GAS  HOW  =     3161299V SCFH
                                                 (WET)
  TIME
  0.
 20«
 404
 604
 80t
1004
1204
'.A04
1504
            MOLC FRACTION S02
              O.OOOOOCE 00
              0.110000E-03
              O.IJOOOOE-OS
              0.210000E-0;!
              0.270000E-03
              04310000E-03
              C4320POOS-03
              C.330000E-03
AVERAGE  RATE OF S02 SORPTHiN
         SAft' t'K 'ji'AniJA- tip
TO
H2SG(, LOADING
CMS ACID/CM C

 O..OOOOCOE 00
 CU3543S2L-C1
 0.701126E-01
 0.10J5'»6E 00
 0.140294E 00
 04174003E 00

 0.23969E-: Op
 O.J5S963E 00

 0.169H5i:-02
                                                     0.1V75.'i?.-;2
                                                     0. 17; S "j;'.--02
                                                     0.170o:SC-C:
                                                     0.166'lTtE-OJ
                                                     o.l6-r.'iu--:2
                                                     o. i6jo^::-:.'Z
                                                     Ot
                      S02 SORf'TJON  RATE
   SA-6
   TFMPERATUHE  •  2004000030 f
   SPACE  VELOCITY .    0.601045E 04  /HR
   INLET  S02  COLE FRACTION (DRYl «     0.002640
   INLET  H20  MULE FRACTION -     0.007703
   INLET  OXrCiPfi MOlf- FRACTION -    0«03'-lp6
   INLET  C02  MOLE FRACTION •    04000000 !
   INLET  NO HOI.f: FRACTION -    0,000000
   INLEi  INERT  CAS KOLE FRACTION -•     0.905-J66
   INuFT  CARBON WEIGHT  «   204720001 CMS
   TOTAL  GAS  FLOW »    7.329909 SCFH
                                                    3  5 71
                                                    (WET)
                                                               0.002487
     TIME
     Ot
    15t
    304
    404
    804
   1004
   120(
   1404
   IfrO.
   H04
              MOLE  FRACTION SOZ
                 O.OOCOOOE 00
                 0.67:>eOOr-03
                 0.£.OC'00'of-03
              p.saocc/of-03

              04120000E-02

AVEHAGE RATE  CF  $02  SOSPTION
                                     H?SO* LOADING
                                     GKJ ACID/GM  C

                                      04000000E 00
    Ot112i!U7f 00

    0.167i.r/l' 00

    o.2i;>6'.tai-: oo
    042366VOE 00

    04127-.45E-02
10 A
                of  /S.'l &M) Acti>/(?n C  -  C./A3E-02
                                                   RATE OF H2J04  tORF'TION
                                                      GMS Acin-'CM C-^a KM
                                                           0. 13670 1;->1J
                                                           0.121C •/•/."••02
                                                           O.ilOi'.'.S-OJ
                                    81

-------
                    SO? SORI'TION  »AU
 SA-7
 TEvPF,.''CTION "    0,000000
 INLET IMrm  GAi KH L FRACTiC'; •     0.6776*8
 INLtT CAkl'.ON Wl'Il.HT  •   62.KI0006 GMS
 VOTAL GAS I LOW  «    20.02
Oi 128CCOF-02
0.12COOCr-02
0.129000O02
0.130000E-02
OF 502 iCRPTION
(If SopfriOfi> vf
of !?.₯ 6MS /kip/
y VtU-KITY ="'
O.OOOOOOE 00
0.245902E-01
	 0.&021S3E-01 	 —
O.S'j5201!-01
0.''OB250F-01
— 0.867062E-01 	 	
0. J03227E 00
Ci 1 200-H" 00
• 0.136V11E 00 • •• •
0.153753E 00
0.1V-0')66E 00
0.810709E-03

fc/ti c = 0-0tl&-0l &M
[yft \— v "
1.50 -ff/itc - -
O.OOOOOOF 00
0.79'-060['~03
0. 76W4**5f -03
0.7620«.1C-03
0. 7()8t*(* S>C*'0>
O.fll967'^f-03 - 	 	 	
0.832'.(!2C-03
0.8269r-03
0.83B886E-03
O.B32<.82i'-C3


S /lOI/S/H C - ftl/V


    5A-0
                    20?.000030 F
    SI'ACF Vf.LDCIlr  =     O.'^3a9'.9l  P/f  /Hi?
    INIF1 502  *LllE  F'lACTI'JN IDRV>  »     0.002800
    INLTT H?0  «OLf  rRACTION «    0.060!,7a
    INLFT OXYGIH  VQLF  FRACTION «    0.03<.gl5
    IHLHT C02  "OLC  FPACTION «    0.000000
    INLFT NO MOIF FRAfTION •    0.000000
    INLET INCRT GAS '•'OLE FRAtTION  '     0.90)716
    INLET CARBON  WEICSHT »   B2.P60000  G^S
    10TAL GAS  FLOW  •    2B.V22999 SCFH
   (WET)
              0.002630
1 |KF

0.
20.
'40.
60.
60.
100.
l?0.
UO.
160.
IPO.
200.
220.
240.
2(,0.
283.
300.
320.
3'.0.
MOLF
	 _.. .
0.
0.
' "~" 0.
0,
0.
0.
0.
0.
p.
0.
c ,
0.
0.
0.
0.
0.
0.
0.
FRACTION S02

OOOOOCF 00
fioooor-o'3
160000E-02 	
205000L-02
?C'.OOOC-02
20:SPOO!:-02 	 —
2c(»000f-02
2060POi*-0?
20^000f--0? 	
2000POI -02
2120POC-02
2) 1000T-02 • '•
22'jOPOC -02
2?'JOOOI -02
230000F-02
2 320POt:-02
2370001-02
2<.'(000l>02
H2S
G'«
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
0.
D.
;j4 LOADING
ACItJ/GM C
dOOOOOC 00
336f."-01
H9'491(.f:-01
9948P1F-01
109468F 00
119<-57f' 00
129243F 00
138624E 00
U7397F 00
10t>2V4f 00
16 2 4'* fir 00
1692&1.F 00
1758 /ft" 00
1B702PI 00
lU73'j!L 00
RATE 0
°us
0
0
0
0
0
o
o
Q
... 	 g
0

— 	 o
0
0
g
0
0
• • — o
F H2SCX. SOBI'
ACIO/G" o"
.UOOOUOE 00
.U577PE-02
.009879C-03
.'.'061 '4F-03
,i06l /'if -03

,'.99<./Dr -03

,
-------
                       APPENDIX A-5


  S02  SORPTION  STUDIES  IN 6"  DIAMETER FLUID BED ADSORBER


                                                        Page

1.  Experimental Results of S02 Sorption Runs  and        84
      Material  Balances

2.  Calculation of Rate of Sulfuric  Acid Formation       88
      from Runs in Continuous Fluidized Bed Unit
                             83

-------
             APPENDIX A-5-1

EXPERIMENTAL RESULTS OF S02 SORPTION RUNS
          AND MATERIAL BALANCES
                  84

-------
   RUN NUMli:U   SA-?l
   UAH     6   » 71
                                 CARIJON
                                              9632'..
  'I Nil  I'  ". '.mill".  i,(i t. Ai-i'.nn
   niiiii i  ;.  MIM iii'.  D,J  r.Ai'i'.iiiJ
    INI I  i  MI/  iDAiilNr, IIM  (.AKhti.i
  "OUT 1. 1 I  Ml/  I.CADIUG  O.I CAI'dfrV

   S02  CON!CI?n RATION  IM  INLFT GAS =
  I.SOX  CDNCfNlKATlUN  IN  I HJ 1'LCT "GAf. -"'
                                              o.'iO  1.
                                              '•,,''•  -•:.
                                           o.o     i r.'i  ;.i)//i u  c.
                                           O.lUfV l.i.S  C,II,VL;1  C

                                                2009. PPM
                                                  16',. PPM .........
   .VULUMl: X  H2II j=  .13.0  X ' "  -:- '• .   :f
   " VuLUFtf 'V"u/"~=' " ''n"2"'i' '   --•—- ..... —----
   CUMCEiaRATIUN OF ,MO=       150.0  PPM
  " TOT AL'7; AS  FL"0-A~RATF== ---------- IZf STf
  U INl.AK GAS VLLOC1TY  =  .. :-;:,;;;-' \?
                                          \- v/ St?C.
                                  200VO
   "TOTAL '.r>PACr Vrt Of. ITY -• •
                                         . " 171'fR .
          S MII i uii.  UITO "i'  c
'lilJVI I I SO/ l.i.AOIMG MM 'CAKIU1N-- ......  "O.PtYj.T  I! US  'S0?/l.!i  C
                                             ;}')'. 6.  PPM
                                             1101. 'PPM
 S(J/  r.LHCrfJl !'.AT IDN  IN  iriLPT GAS "
 Sl,>  Ciii-iCf. Ml i< AVION  [M l,UTl.i;-T  C,AS"
 VIM UMI  '!!  H.'-'il  -'  1 ^.0 '(,
'VU.llH!  '..  I!/'   -   'i .^. K
 ClifJl.l.i^TK'M I (li-l I.I I-   N(J-

"TUAI.  ;;AS  ii.ir/j  KATI:.-=
 t. Ml AK C^S  v/l.ldCIIY

1 Tl'.,v|'t-i',AIUKr       "  -
                                   ?..<' FI/SI.I

                                  l.O DTCT "
"TUI Al.
             i; v/i:f.tiC'lTY ' ='
                                 3')Tr).  "17KR
 p (Hii-i LI s su L i u i<  i n r tj "u r'Ac r o ';<
    Nns SHU-UK  HUT ni: KF
   SUI.fUl;  ACCOUNT f-0  I-UR"
                                        OT'i i '.7  t TI s / i
                                        o.3a/)»

                                        "  "9?..3' 31"
                               85

-------
  rul I I.K i Al.  ll/VL/vrll.l  I'UK  Ml/ :>lliP'ACf. "VL'YOC 1TY"  -     ";s« VI ." T'/illl
               u "ifjiu Ki:AcTtfK' ""=    ""0". 2T;:o "t oS/n,^"
         SULTUK our  oi: KL-ACTOK-     0,203?  LBS/HR
   MAIbKIAL  IlALANCt  FOR S02 SORPT10U
  KUM NUK'BfK   SA-2't         CARQON
  CATC    6 16  71
  PUII I  T  4 SUI.FU'v flN  CAUiif'N    i       ^,'i't  -:',
 MNLM  S()2 LUADIIjr, ON CAKl'OM -     0.0     LBS  Si)2/L»  C
 "cun.i;T  sn2 LOADING  ON CAiunw-'-^onzjo  LIIS  so2/L!rc

  S02 CliiJCL'NTHAl KJ'I IN IMLIl  GAS  -       391)2. PPM
 ' S02 CONCrNTRATIO-l IM aUTLIT'OAS-  	  I'O?:!. PPM

  VIILUMI  •;; 1120  =  I3.o  •;;              .  V ..  •
  ViiLUI-'l:  o 02   :-   't./i'Z    	""    "	~         '	.-..:•..
  CO"IC.[ Nl'RAI ION Ol: ,N(J=      150.0  PPM

 'TOTAL GAS TC'OW  «'ATI.:="  	O6'i ."IV'S'CTIi	~"   	-	-	
 : I. I NF \'\  ;, AS  Vf I.('•(, I I V  •.--       • 2 .0 'f T/ Sl;C

 ~Tf>'Pl RATURT         =-•-  -2TO.'


 '.TOTAL  sPAct: "ycLucirv  --       n,
'POU^CS SULIUR  I,'-iTO KI.'AC'IOK  " 7--"":'  ' U"; •l'>r.T"l l-"/(,R
 POUNDS SULLOR  UUr  Ol-  KfACIdR-     O..U'.6  LUS/IIR
 't si/11 UK A('.COOMI!:I! I-HR

-------
  MATERIAL BALANCE FOR  SQ2 SORPflOM
 RUN  NUf-'nFR   SA-25        CARBON      9612't.
 DATE    6 17  71
       '«"'sUt>'UT<"OM~'C"ARunrr^'"~«"' --------- lyr'nr^-- — - — "—•
IOUTLKT  s SULFUR ON CARBON   = ::,    4.02 •«          :
r INLET  SOP LOADING ON . CARB'UN * ?':' < 0.0-'  l.tiS • SOZ/Lft C
"oo TL e t ' SOT TO AD i HG~IW ~rAr:.^:i::' b.;j7. %   -:  '":'••' •:'"•"•
? INLI'T  S02 LUAUING OM CARBO'M. -.". '- •'•• 0.0:' :>; I.B5 Sij2/LB C
"OUT LET  SC2"LOAinilG ON"C'ARTJaN='"":: ..... 'O^TZt'O-T 3S"-Sa2/TiI C
 SC2  CC.NCENTKATION IN IMLE'T  GAS =      20^>0.  PPM
   2- CONCENTRAT 1 OM" 1'IST T'UTLEr^GAS^;;;"-"- -/i'6-.— PPH
i: VOLUME  ^ H20  -  13 . 0  -''.^l
'•VCL'UMir .:; •02"""'^  ^.3"^      '    ....-^-.
 CCMCENTRATICN  OF N0=      150.0 PPM
TT G T A L' G A'S~nTTlW~ R'A T F=	   1TB S7 U ; SC
JLINFAR GAS Vi:LOCITY =        2.3 FT/SFC
"T EMP'il'K'ATURF
    NOS" SULlHjR"  INTCr'rtF AT,T'HR"'"""   OT/T7F L
 POUNDS  SULFUR  OUT  OF REACTOR-    0.2370  LBS/HR
   -SULCUR" ACCOUNTT.o"
                       87

-------
              APPENDIX A-5-2

CALCULATION OF RATE OF SULFURIC ACID FORMATION
   FROM RUNS IN CONTINUOUS FLUIDIZED BED UNIT
                   88

-------
  CALCULATION OF RATE  OF  SG2 SDRPT10N  FROM
            FLUIDIZEO  BED  RLACTOR
 RUN NUKliF.R   SA-21
 OATh    6   8 71
                           CARBON
5 INLET %  SULFUR OM C ARBON ': •>:.- .
?CUTLEI_ %  SULFUR Ofj CARBON' '""'=-.
""INLCT ~$02"'TOAi)TMO~ ON"C"A'fU$0'r^r
 CUTLET SU2  LOADING DM CARfJOM=
96324.
                                   T. 23' :;r"''5- -;:;''-
                                   "OT'O"" ---- \TDTS' '5G2/L1VT.' ""
                                    0.1168  LBS  S02/LB C
F'S'0'2 CONC t}'iTiTA"T I ON 1 ,N
|SG2 CONCENTRATION  IN OUTLET  GAS=
                                          164.  PPM
                            1'50.0 PPM
 VOLUME  .10?   =  4.2
 CONCENTRATION OF .M0~
i TOTAL GAS  FLOW RATE=.:/-:.::;i:: 12^9. 0 ;.
I; LINEAR GAS  VELOCITY:^ f^    2.'*  FT/SEC
 TEMPERATURE
                            200.0 DEC F
! TOTAL SPACE
AVG
LBS
* STAGE
r
2
3
4
5
6 ,
7
8
P- "i f:t Wt &
ACID LOADING AVERAGE S02 AVERAGE RATE OF
H2S04/LB C CONCENTRATION ACID FORMATION
0.0213
0.0426
0.0662
0.0920
0.1480 ' .
0.1817
0.2266

PPM LbS H2SH4/LH C-HlN '
251. 0.00076
42t>.
607.
808.
10 Lei.
1247.
1507.
1827.
'•• W:-'\' v'.y^k-:^""1' :-!-:'';::'v ::-::' :••'!•/ :'.•:•*' •
••'• ,'•'. :'.-::.'.'::'..: ;: '•'. •'•..': .-.:. • . '. > ;..' '. •• ':•';'• '
0.00076
0.00084
0.00092
0.00092 	
0.00108
0.00120
0.00160
;?;•::. :'-::^':0'.r :'v.':, •;>••': ?-:/-:: •:-'-•: '*-i?\
 OVERALL RATE  OF  ACID FORMATION  =
                                         0.10113E-02
                             89

-------
  CALCULATION OF RATE OF  502 SOrtPTION  FROM
             FLUIDIZF.D BED  REACTOR
 RUN  MUMMER   SA-22         CARBON      9632'f.
 CAJF.    6_ 16  71	^	   ___	^

i INLET v,  SULFUR ON  CARBON •. \--= 'v' •'•• •'.':./ 6 .40' "% '"•,;••';-'. \'":.;-:^.:'^::,:'\';-•
;• OUTLET '*  SULFUR ON CAR30H -'l^'feW; • • AVtjT.X -';"l_"':'"'"' :?'''V 'v'::'.:' ' '•
"iNLl-'-T ^02 "LOADING "ON" CARtic'N ="J  oTo  "   QTs so?7LB"c"
 OUTLC-T S02  LOADING-ON CARBO,M=     0.1.468 LBS SU2/LB  C

F'SU?: "fCj.N.C'il'NI 'RAT IOt.!'"rir"i"NLF.'T" GA "$""="""/ ~TOV6"7""PPM     '.	
! $02  CtNCtiNTKATION  IM OUTL I.T.. GAS=   ;'  <  11 !il . PI>M

"vOLOi'.'i- :'.;"  1120""= 1 i.p""r*    ;--—-—--	-    ,..----.-	—..-
 VOLUf'u K  02   =  /t.2  'S
 CONCOTRATION OF  NO--    _ ir>P«o  PPM      	

? TOTAL GAS FLOW RATS:=,  .  1140. 0' SCFH -  .'".X. V'•-' ::     ':''."
M.INEAR GAS  VELOCITY  =^''_-'JL£^. FT/^ij ,:•:•'  .^ .   '•  ;

 TEMPERATURF          =      200.0  DEC F


[ TOTAL .SPACC. VELOCITY '^}: ;;;;f;'"39's|9/  . I/HRf "?£:;'-'f:.'' '''•.U'-';^;':?';-:'


    '  "   AVG  ACID LOADING,    AVERAGE S02    AVF.RAGE KATE OF
         .LB$_H.2Sn4/Lrj _C_    CONCENTRATION   A C_I 0  PORMAJJOM
f"STAGE. v."w;".,;,' -t~::'-,;• J;].:"/::t^-;^:-^:^                     '''C-i^'

                             -'::y^'••••'Q'• ooiL2/Cii'
   2           0."6'"""    Ibl^"""     "^'^"OT06T21""
   3           0.08R8              190't.            0.00113
   /»         _P«li!.lA_       	?21?'	    0.00132
   5"	..""  "bTl!»3T              2'j^j,            OV00123 ""
   6       .    0.187S              2868.            0.00139
   7.  .      0.227/t^	^^'-^	.	
   B"""	    0."2/72""  **~~~~  ~"^    369i>".  "  "
 OVERALL RATE  OF ACID FORMATION  =
0. 13983E-02
                                90

-------
I
  CALCUIATICN  (!F RATF. OF SD2  SLJRPTION FROM
            FLUID17(:D BED REACTOR
 RUN HUFBER   SA-23       CARBON      96324.
 OATL   6  If.  71
 INLGT £ SULI;UR (JN CARBON " ^.:- '":.;' :f: .0,40 -^
 OUTLET ?,  SULFUR ON CARBON  '  = ''" ' ':: :>4 . 9 I X
 1INLL T SU2 "LOAD I N'G "ON CARROiT "="":	"aYTr"^"
 GUTLf-T S02  LOADING ON CARBON=     0.1008 LbS  SU2/LIS  C

 S02 CONCr^TRATION' IN TNI.FT GA$~=	 ~7.W). 'PPM	
           T RATION IN i:un. tl  GAS=     .    0. PPM
 VLLU^L %  02   =   4.2 %
            ICM OF NO-'      1'jO.O  PPM
; TCVAl. tiAS  FLOW KATt":=     1106.0  SCI M
UlAIUAR GAS  VELOCITY -  .;:   2.1  FT/SCC
 TEMPCRATURE         =     200.0  DEG F
 TOTAL SPACE :VEl OC 11Y -      3*341.  1/HR
 STAGE
   3
   7
   fl
AVG ACID LOADING
LBS H2S04/LB C
• E
o.
0.
0.
0-
6.
0.
0.
0.
008 7
0260
0477
0 70 3
O9'j4 "'
1241
1562
1909 	
- ;' ••:•'" V •'>.':-•.;
AVERAGE S02 AVERAGE RATE OF
CONCf-MTRATION ACID FORMATION
PP 1 LfS
46.
183.
388.
621.
1475. :';'"; '',.'-
'""'
^J-^M'-^^^^f^x'^--'
O.OC035
D.OU071 " ~ ~
0.00009
0.00092
'"0.00103 	 """•"
0.00) 17
. 0.001 U


 OVERALL RATE OF  ACID FORMATION =       0.97531E-03
                               91

-------
  CALCUIATION  OF RATE OF S02  SORPT10N FROM
             FLU IIM ZED BED RFACTOP.
 RUM  NUMBTR   SA~2'i        CARBON      96326.
 CATi:    6  16  71
 INLET % SULFUR C)M  CARBON  . ;. ;. = ;:•; •./-. '^Q .40> % •• v-^',-; •;;:• '^'^.^
 CUT LI: f '<  SULFUR ON CA-sOCM  .V - ^ '*;':.. 5:1 M^X " •£ ••; [^ i ^''-'
 I NLL T" SO?  LOADING"ON CA'R'lUJN ""=."   "oro"""   Ui'S "S'027L'(i" "C"
 OUTLET SO/?  LOADING ON CARUON=    0.1230  LBS S02/LO C
 'Sl)2  CONCENTRAT'lOf!  1 N "IMLFV'GAb"=~Z.'"'
 SC/'  CO.\'Cf.:,NTRATlUM  IN OUTLET  GAb'=."'- •: .  10 /«.
'VGl.UMi.  ;j"ll?0 = 13.0  l^  ":	
 VI,I  UMF.  K 02   =  A .6  £
 CIIMCL'VI KAT ION 01"  N0=      I'iO.O PPM
. TtiTAL  GAS  FLO.fi RAIL"= .: :;  96A . 0 SCt;H :.: :•
 L iMEAft' GAS  VELOCITY  =   ; : . ';'2 .0. .FT/StC"
 TEMPERATURE          =      250.0 DEG  F
                r i n r t i \/ —      TO//   1/tiO
         AVG  ACID LOADING    AVERAGE  S02    AVERAGE  RATt OF
          LOS  HZSO't/LB C    COiJCF>jTRAT ION   ACID FORMATION
fSfAGif " .." •,  '  :.-::'"'' vi^-^B:•:>:"' """T-;"lP>M^^v:;:':O-Li3^n<2S"TjV/"LC7'C-n.
   2           O
   3           0.0730              L795.            O.OOL02
   A    _     _0_. 1002   _____   _?_l?J_*  ____   _ °'001013
   S" .....  """ ""0.1282 '"••".' .;.;:•". .'^~"  2^70^ :••:;•;; -  .~T "o;ob)'ll'
   6      "    0 . I 'i 3 0 :  :'" •••• • ' ••• ; ••- -.-. / -: •'. : 2 7 3 1 v *&•£>:. ""/'"" 0.00099.
   7          _°           '    ''"
   8 ........  "•'" ..... 6
 OVERALL RATE  OF ACID FORMATION =       0. 12288E-02
                                   92

-------
I
I
  CALCULATION OF RATH  OF  SU2 SORPTION  FKOM
            FLUID1ZED  BED  REACTOR
 RUN NUt'BER  SA-25        CARliON      96324.
 DATE    6  17 71
i INLET  -X  SULTUR ON CARBON ";   =       0.40 S     .:;}-•..
'ouii.nr  *. sui.ri'R ON  CARBON   =_      4.0? %    ""•'•",.."
"IW.I.1  SOyTuADI'JG ON "CAlU!'0;-J~="    "C'Yir~'~TfeS''~S'02'/LIV "C"
 OUTLET  SG^ LOADING  ON  CARBOM-    0.0837 LliS S02/LB  C
                     IN  RL CT "GA"S""=' "rT"~-7D7&." PPM'
     CONCENTRATION  IN  IJUVLTT GAS = :;/:^. V'v4 11 .  PPM
' VOi.UMif ^
 VC'LUf'.lI  %  02  =  4.1  ^
 CLU(;t:i\TRATIGM OF N0=      I'iO.O PPK
 TOTAL  GAS  FLO-V KATt=     1 09'j . 0 .SCFH
 L INF. AR CA   V12LOC 1 TY =        2.^
 TCKPFRATURE        =      250.0 UEG  F
STOTAL  SPACF VELOCITY  -      38(v.  I/HR
         AVG ACID LOADING    AVERAGE  S02    AVERAGE RME  OF
          LBS H2S04/LB  C    CONCENTRATION  AC10 FORMATION
STAGI
1
2
3
4
5 ;: : . ;
: 6 i:/v:'': .,'>
7 •:. ":..
8
0.0140
0.0307
0.0464
0.0657
' O.Oi',32
0. 1043
0.1279
0. lb!31
434.
*~ "6"44T
813.
996.
lid/.
1 i»J6.
1621 .
18b6.
                                                 O.OCO'j6
                                                ~0~T)'0'U6T
                                                 0.00063
                                                 0.00077
                                                 OT'OO 0 TO
                                                 0.0008^
                                                 0.0000'j
                                                 DTO'OTG'9"'
 OVFRALL RATE  OF ACID FORMATION =       0.77687E-03
                                93

-------
  CALCULATION OF RATE  OF SC2  SORPTION FROM
            FLUIDIZEO  BED RtACTOR
 RUN Nl)f-T>l:R  SA-26
 UAH    6  18 71
CARBON
96324.
; iNLi-.i  '.r.  SULFUR ON  CAIUWN '   •=  \:. :
lUuriH  '-.; SULFUR ON CARBCN  .'=":•>:"
"iflLLT  S'G2" LH'AUfNG  UM CARlWi" ="*"
 UUTLI. r  SU2 LOADING ON CARBON=

' St)2 CU\C'!:>n RAT I OM  I N I f-OT~ G'A'S" '="
; SC2 CUW.iiNT RATION  IN OUTLET GAS =
         ~ff.~o	CTnrsDz/Ui  c
          0.1210  LliS  Sd2/LB  C

         ._	705'i; "PPM	'"	
'VULUMt.  :;\ H2C'"-" l"'j'.U~'
 VCLUMf  i 02  -  4.3
 C L N C I: N r K A V i Ij N  0 F  \ U =
 LSO-0  PPM
* TOTAL  GAS I-LOW R ATE=  ', ,"1 168 .:0. :SCFH. "-^:
J L INEAR GA-S. VtLOC I TY .="'"."I/:;,,:>;: i ,2'2 .;3;.
 TtMPtRATURE
; TOTAI  SPA'CF VCLOCITY -
 200.0  DEG F
       t>.  l/HR

STAGE
1
3
4
5
(,
7
U
AVG ACtD LOADING
LtJS II2S04/LB C C
^?oJo?7V;S^S
0.0377
0.0583
0.0817
" 0.1068 ..." '
0.1346'
0.1660 •"•:: :-:•'• :
0.19/4
AVERAGE SO
.ONCF..NT.UTI
••fpf>.;vl'5.2:i-'e
324.
S34-
758.
1003.

2 AVERAGE RATE OF
ON ACIO FORMATION
•.,v|p;;i ;vyv :.:• :•• : 0 ; 0 0 0 y 2 ;• ; . ;> !;. 9; ; .- ^: ;.
~^ ' "DTO'OiTbF"
0.00088
0.00099
:::;y'::'";.-':^ .0.00110 ' -t\.'
:;;fe;;":;::'V':;'...0.00133 "-••• .:• •".'"
0.00133
 OVERALL  RATE OF ACID FORMATION =
                0. 10476E-02
                               94

-------
        APPENDIX A-6





MULTIPLE REGRESSION ANALYSES
               95

-------
  DIFFERENTIAL BED DATA -  EFFECT DF  VOLUME FRACTION OXYGEN ON RATE
  RUMS 138,139,144
  VARl = LN 02
  LMRATE/I 1-LOAOING/.38) )
  VAR( 1)=-0.400088E  Oi'f  VAFU  2 ) *-0 i70a355E 01
             ''
  SIANCARD DEVIATTniM^
  VAKI 1>= 0.647692E  00,  VAR(  2)= 0.409425E 00
^SIMPLE CPRREI.AT iriNi  r.npFF i f-l FNTS
  VARS( it  n*  o.iooooe  01,  VARS<  i»  2)= o.98395£ oo

  S TEP Ml.lMRCft   <           FMTii.B A/A3 1 A^f g _ l'
  STANDARD ERROR  OF  ESTIMATE=  0. 7345897E-01
  R SQUARED =  0.9681584E  00
 _ GOODNESS QP  FtT.FI .   It   f^l)= ..... n.?7ft^QO?F Q4
  CONSTANT TERM * -O.<.59506*£  01        AMTJLOG CONSTANT TERM =  0. 1010158E-01
  VAR      CQEFF         STO D£V    T VALUP     BETA COEFF
    1   0.62198E 00  0.118245E-01     52.6013   0.98395E 00
DIFFERENTIAL  BED  DATA  -  EFFECT OF VOLUME FRACTION V»ATER  ON  RATE
RUNS  157,139,160
VAR1  =  LN H20
VAR2  =  LN1RATE/I1-  LOAD ING/.38))
AV^AGFS			
VARI  1J=-0.234333E  01,  VARl 2>=-D.708523E 01
VARI 1)= 0.^^1023E  00,  VAK(  2)= 0.337632E 00

<;IMPI F r.riRRFiATinrj  r.
VARSI  It  U=  O.IOOOOE Olt VARSI L, 2)= 0.9^259E 00

     'NUHBPg.  I  .................. eKrE»..VARl.ARLF  I
STANDARD ERROR  OF  ESTIMATE=  0.1032892E 00
R SOUARtD =   0.907^175E 00
       «; nF  FITTF>    if  92)=
COMSTA:>4T TERM  = •  -. 537632511 01  :      .ANTILOG  COf4STANT  TERM *  0.^62 s:;;; •  STU o=v  ;  :T VALUE     BETA  COEFF
            '       "'
  1   0.72927E  00  0.242858E-01    30.0265    0.95259E 00
                                       96

-------
 DIFFERENTIAL BED DATA - REGRESSION TO FIND ORDER OF S02
                         AND LOADING WITH ORDERS FOR H20 AND 02
                         FIXED FROM RUNS I AND II
 RUNS 139,140,14 ItI42t143,148,149,150,151,152,153,158
 _VAR1 = LN S02	
 VAR2 = I/TEMP                    "                             "
 VAR3 = LN(RATE/(l-LOAD/.38HH20**Mn02**Pn
 AVERAGES	,	_._	. .	
 VARJ 1)=-6.659038E  Ol7  VAR(  2J=  0.152275E-02, VAR (  3)'=-0.2944826 01

 STANDARD DEVIATIONS            	
 VAR( 1)= 0.627714E 00,  VARl  2)= 0.119787E-03, VAR{ 3)= 0.856011E 00
LSIMPLE^CORRELAJION COEFFICIENTS
 VARSJ  I, 1»= O.IOOOOE 01, VAR'Sl  1,  2>=  0.14132E  00,  VARS(  I,
 VARSt  2, 2)= O.IOOOOE 01, VARS(  2,  3)=  0.80794E  00
; STEP NUMBER  1           ENTER VARIABLE  2
: STANDARD ERROR OF ESTIMATE3   0.5050560E 00
_R SQUARED ~ __p..6.5277_2lE_00	:	
 GOODNESS OF FIT,Fl    1,  3~92)=  0.7369407E 03
 CONSTANT TERM = -0.1173662E  02
 VAR      COEFF  	   S,TQ_QEV
                                        ANTILOG CONSTANT  TERM
                                   T  VALUE      BETA  COEFF
                         COEFF
       0.57736E 04 0.212683E 03
                                    27.1467    0.80794E  00
                                                                   0.46« 00
                   0.7995579E-05
  STEP NUMBER  2           ENTER VARIABLE  1
  STANDARD ERROR OF ESTIMATE=   0.4065425E 00
 _R_SQUARED_?	0. 7755923E  00	
  GOODNESS OF FIT,F~(   2,  391)=  0.6756807E 03 :
 CONSTANT TERM « -0.8010632E  01
 VAR      CQgFF         STD  DEV
                                        ANTILOG  CONSTANT  TERM
                                   T VALUE     BETA  COEFF   ;
                   0.3319150E-03
                        COEFF
   1   0.48276E 00 0.330011E-01
__ 2. __ ja*
                                    14.6287
0.35401E 00
0.7579IE 00
                                       97

-------
 DIFFERENTIAL  BED STUDIES - REGRESSION  TO FIMD ORDER OF SOZ                   III
                             AND LOADING WITH  ORDERS FOR H20 AND 02
                             FIXED FROM  RUNS  I AND II
 RUNS  139,1401141,142.1431148,149,150,251,152.153.158
_VAR1  = IN_S02_ _ ,
 V-AR2  * I/TEMP            -.        ,•:•>•„,' v.v ..-  :  ••'   ,   :• .-. .'•<••.••!.'•<•„.:  ':•«..-.  .-:•>   .'.
 VAR3  * tNIl-  LOADING/. 38)       v • • •• VxV"'- •"::'~;v:'.. •"•' ^V'X' •''*••• "': •''•'-'>: . 1?-''-''".',:'-i ..;•• '
                                        '  '          '     '            •   •   "
 AVERAGES
 VARI  1I=-0.659038E 01, VAR( 2)» 0.152275E-02,  VARI  3I—0.253406E 00, VARI  41— 0.319822E 01

 STANDARD  DEVIATIONS    ~~        .       ~                          ~  !
 VARI  II'  0.627714E 00, VAR( 2)> 0. 119787E-03,  VARI  3>- 0.272UOE 00, VARI  4)* 0.912883E 00
 SIMPLE CORRELATION COEFFICIENTS                                                                     '  •
 VARSI  1,  11=  0.10000E 01, VARSI l,'2l«  0.14132E  00,  VARSI 1, 3I*-0.15079E  00,  VARSI 1, 41- 0.38742E 00
_₯.ARS|  2j_2)-_0.1000.0E_Qlt-JMBS.( ..2,.J.L«r0. 1B505E  00.  VARSI 2. 4)' 0.70257E  00	
 VARSI  3,  3)-  0.10000E 01, VARSt 3» 4>«  0.351476  00

_SJ£P...NUMBER_J	ENTEB. VARJLABLE	2_
 STANDARD  ERROR OF  ESTIMATE*  0.6504441E  00
 R SQUARED -   0.4936111E 00
,OOODNESS_OF. F1T.RI	It.. J92J_« _..Q.*3.821084.E_Q3	,	„__
 CONSTANT  TERM • -0.1135137E 02         ANTILOG CONSTANT TERM »  0.1175337E-04
 VAR       COEFF        STD OEV    T VALUE     BETA COEFF    ,.    • >
	:	CO.E£E	,	,	       :/'; •...-><.,;, : .  '.  "
   2   0.53542E 04  0.2T3907E 03    19.5476   0.70257E  00

 	ENI£fi_«A)UABIJE	3_
 STANDARD  ERROR OF  ESTIMATE-  0.4723298E  00
 R SQUARED «   0.7336542E 00
         t  np  FIT,FI    ?.
 CONSTANT TERM  >  -0.1199815E 02        ANTILOG  CONSTANT TERM «  0.6155597E-05
 vAR      COtt-f        b)U UtV    T VALUE     BETA COEFF
	COFFF.    	             	
•   2   0.60573E 04  0.202397E 03    29.9278    0.79483E 00                  ,: *
£ '/J.   0.16726E 01  0.890985E-01    18.7720    0.49B55E 00           .. ,  , '  '^, ..

 STEP NUMBER  3          ENTER VARIABLE  1
 STANDARD ERROR OF  ESTIMATE'  0.3417416E 00
_a_SflUAREO_«	O.B609285E_00._		
 GOODNESS OF  FIT.FI    3, 390)-  0.8047700E 03         .         --'•--   ,Jv: V;>
 CONSTANT TERM  «  -0.7980425E 01        ANTILOG  CONSTANT TERM -  0.3420941E-03
                  	STD DEV    T VALUE	BETA COEFF              : .
                         COEFF
   1   0.52844E  00  0.279714E-01    18.8922    0.36337E 00
  _2	0.51121 E_D4_0.147.447£_flL3____JL8...ILZ5-5	p.75216E 00
   3   0.18299E  01  0.650004E-01    28.1518    0.54S4SE 00
                                                  98

-------
                        APPENDIX A-7





COMPARISON OF MULTIPLE REGRESSIONS TO DIFFERENTIAL RATE DATA
                             99

-------
                                             MODEL A
RATECU I = COEFF *  11-X( I >/XS)**A *  (YS02**B)  *  (Y02**C)  *  (YH20**D)
   WHERE COEFF= K * EXP(-F./R* (I/(T+460) ))

        T=    200.         XS=    0.38      YS02=  0.00200        Y02=   0.007      YH20=   0.100
     -E/K=   5520.         A=   1.000          B=    0.400          C=   0.630         0*   0.730
        K=0.000159
                                             MODEL B



fUTFCII 1 = COF.FF * U-XII)/XS)**A * (YSQ2**B> *  (Y02**C> *  (YH20**D)
   WHERE  COEFf= K * b'XP (-E/R* ! I/ U+460 ) 5)

        T=    200.        XS=    0.38      YS02= 0.00200       YCI2=    0.007       YH20=   0.100
     -E/R=   5416.    ,     A=   1.000          B*   0.480 "        C=    0.620          0=   0.730
        K=0.000332
                                              MODEL C


RATECIU'COEFF  «  ( 1-XI I )/XS> **A  *  (YSC)2**BI  * (Y02**C) * (YH20**D)
   WHERE COEFF= K  *  E XPC-E/R* ( L/(T + 460M )

        T=    200.         XS=    0.38      YS02= 0.00200       Y02=   0.007       YH20=   0.100
     -E/R=   5732.          A=    1.830         B=   0.530         C=   0.620          0=   0.730
        K=0.000342
                                            100

-------
            FU3 HUMBED » 138-G
                                          21 71
Xt.IltGKS HZS04/GM C    RATE, GMS H2SC4/GM C-NJN
0.0024220
0.0017513
0.0012296
0.0008421
o.ooo&ies
0.0005291
0.0005068
O.CCC4918
1.0004844
O.OC04770
0.0004620
0.0004546
0.0004397
0.0004243
0.0204173
0.03040S9
0.0003987
0.0003913
0.0003875
0.0003801
0.0003763
0.0003726
0.0003689
0.0003689
0.0003652
O.C003652
0.0003615
0.0003577
0.0003540
0.0003540
O.OC03540
0.0003502
      _
       O.CC290
       o.co<.;5
       0.005BO
       O.C07.->5
       0.00870
       0.01015
       C.01160 '
       0.01305
       0.01450
       0.01813
       0.02175
       0.02538
       O.C2900
       0.03263
       O.JS625
       O.G3988
       0.04351
       0.0*713
       0.05076
       O.05438
       O.C5801
       0.06163
       0.06526
       0.06888
       0,07251
       0.07976
       0.08701
       0.09426
       0.10151
       0.10876
       0.11602
                                [MODELJl]

                   CALCULATED RATE.  GKS H2S04/GH C-HIN
0.0004622
0.0004604
0.0004567
0.0004569
0.0004551
0.00'J4S34
O.OC04516
0.0004498
0.0004480
0.0004463
0.0004418
0.0004374
0.0004330
O.OOC4286
0.0004241
0.0004197
0.0004153
0.0004109
O.O004064
0.0004020
0.0003976
0.0003932
0.0003887
0.0003843
0.0003799
0.0003754
0.0003666
0.0003577
0.0003489
0.0003400
0.0003312
0.0003223
                                      [MODEL B]

                         CALCULATtO  RATEt OHS H2SC4/GM C-MIN
 O.OOOS268
 O.OOC5248
 0.0005228
 0.0005207
 0.0005187
 0.0005167
 O.POC5147
' 0.0005127
 0.0005107
 0.00050E6
 0.0005036
 O.OG049S5
 0.0004935
' O.OOC48S5
 0.0004834
 O.C004784
 0.0004733
 0.0004683
 0.0004632
 0.0004562
 0.0004531
 0.0004481
"0.0004430
 0.0004380
 0.0004330
 0.0004279
 0.0004178
 0.0004077
 0.0003976
 0.0003876
 0,0003775
 0.0003674
                                        [MODEL C]

                           CALCULATED RATE. CMS  H2S04/3* C-HIN
 0.00064CI
 0.0006357
 0.0006112
 O.C006267
'0.0006223
 0.0006179
 O.OOC6135
 0.0006091
 0.0006047
 0.0006003
 0.0005895
 0.0005787
 0.0005680
 0.0005575
 0.0005470
 0.0005366
 O.OC0526J
 0.0005160
 0.0005059
 0.0004959
 0.0004859
 0.0004761
 0.0004663
 0.0004566
 0.0004471
 0.0004376
 0.0004189
 0.0004C05
 0.0003826
 0.0003650
 0.0003478
 0.0003310
                                                      MEAN DEVIATION -    0.0000186    ROOT MEAN SQUARE  DEVIATION
                                        [MODEL A]    " RESIDUAL  SUf* OF SQUARES  = 0.128506-07
                                                      MEAN PERCENT DEVIATION •>   4.4846649
                                                                                                                             0.0000222
                                        [M03EL B]
                         MEAN DEVIATION «    0.0000531   ROOT MEAN  SQUARE  DEVIATION
                         RESIDUAL  SUM OF SQUIRES  =  0.85176S-07
                         MEAN PERCENT DEVIATION -  13.5773V26
                                                                                                                             0.0000572
                                                       MEAN DEVIATION  =   0.0000939    ROOT MEAN SQUARE DEVIATION
                                        [MODEL C]     'RESIDUAL  SUM OF SQLHRES - 0.27103E-06
                                                       MEAN PERCENT DEVIATION  =  22.8247833
                                                                                                0.0001021

-------
     RUN NUMBER « 139-0
                                        U 2? 71
MlltGMS HZS04/GM C

       0.00294
                                      [MODEL A]

RATE, CMS HZSC4/GM C-M1N   CALCULATED RATE, CHS H2S04/I.H C-HIN
            [MODEL B]
CALCULATED RATE, GHS H2S04/GH C-HIN
                                                                                                                               [MODEL C]

                                                                                                                  CALCULAtED'RATE,  CHS HZS04/GM C-N1N
 0.00589
 0.00736
 O.OOB83
 0.01039
 0.01177
 0.01)24
 0.01-.72
 0.01839
 0.02207
0.02-143
0.03311
O.C3->79
0.040*7
0.04415
0.04783
O.UM51
0.05r>18
0.058B6
0.06254
0.06622
0. 06-190
0.07J58
0.08094
0. 08830
0.0'V>65
0. 10301
0.11037
0.11773
0. 12f.09
0. 13244
0.13980
0.14716
0.16168
0.17659
0.19131
                             0.0070602
                             0.0051134
                             0.0037625
                             0.0021232
                             0.0012E57
                             0.0010750
                             0.0009443
                             0.0008716
                             0.0003203
                             0.0007699
                             0.0007627
                             O.0007462
                             O.0007409
                             O.0007336
                             0.0007264
                             0.0007191
                             0.0007118
                             0.0007046
                             0.0007009
                             O.OU06936
                             0.0006900
                             0.0006864
                             0.0006627
                             0.0006791
                             0.0006755
                             0.0006683
                             0.0006610
                             0.0006538
                             0.0006465
                             0.0006356
                             0.0006247
                             0.0006138
                             0.0006028
                             0.0005B83
                             0.0005775
                             0.0005464
                             0.0005230
                             O.OOC4903
                                     0.0008920
                                     0.0006865
                                     o.oooaaso
                                     0.0008815
                                    "0.0008781
                                     0.0008746
                                     0.0008711
                                     O.OOOB676
                                     0.0008641
                                     0.0008554
                                    " 0.0008467
                                     0.0008380
                                     0.0008293
                                    " 0.0008206
                                     O.OCT08U9
                                     0.000(1032
                                     O.O007945
                                     0.0007858
                                     0.0007771
                                     0.0007684
                                     0.0007597
                                     0.000/510
                                     0.0007423
                                     0.0007336
                                     0.0007249
                                     0.0007075
                                     0.0006901
                                     0.0006727
                                     0.0006553
                                     0.0006379
                                     0.0006205
                                     O.OOD6030
                                     0.0005856
                                     0.0005682
                                     0.0005508
                                     0.0005160
                                     0.0004812
                                     0.0004464

s
' *
•
... x *

?

• • , •'•
t '-',/;

l._t__
''•'::.: !•/'•"•, ••
0.0010060
0.0010021 '.'..:
0.0009982
0.0009942 -: -I .- ' :'
O.C009903
O.O009864
0.0009825
0.00097B5 .: -. <
0.0009746
0.0009648
0.0009550
0.0009452
0.0009354
0.0009255
0.0009157
0.0009059
0.0008961
0.0008863
0.0008765
0.0008666 -•- <
O.D008568 .,:;;•....
0.0008470 !r- S
O.OOOH372
0.0003274
0.0008176
^T" 0.0007979" -.-r-'^
', - ' 0.0007783 ., ' :; ;.•:;:•'
0. 0007587 :,..».
0.0007390
0.0007194
O.OOO6998
0.0006801 -'^'/f- :
0.0006605 '"- -'••-'
	 O.OOJ6409 -; ..,,.
0.0006212
0.0005820
0.0005427
> •:••. ••• -. 0.0005035 ••'.. . ••• -••:•
0.0012185
0.0012096
0.0012CH
:" 0.0011925
0.0011839
0.0011753
0.0011668
0.0011582
O.O01149T
: ; 0.0011286
0.0011077
0.0010370
0.0010664
0.0010460
,: 0.0010258
:-\ ."•. :• 0.0010058
0.0009859
. 0.0009662
0.0009467
.. . ; r: • 0.0009274
;., . , ..'. 0.00090B3
• : • •- : , • •-.'• 0.0008893
O.OO08706
O.OOOB520
0.0008336
7V7T' >,"" "0 x' ":'.'" 0.0007973"'
! - -'• •'•'.-:' : 1 0.0007616
i..' .• '.-. :'"•" : ..,; . 0.0007270
0.0006929
0.0006596
0.0006271
.';••... :, 0.0005952
•>il- •;»• .. Oi0005642
,. . -- /... •'•'., , 0.0005339
0.0005043 	 ~"
0.0004475
0.0003938
'; ••;>.-, 0.0003433
                                          KEAN  DEVIATION =   0.0000556    ROOT  MEAN SQUARE DEVIATION
                           [MODEL A]    "  RESIDUAL SUM  OF SQUARES - 0.1S155E-06
                                          MEAN  PERCENT  DEVIATION *   7.6649427
                                                                                                                      0.0000678
                                          MEAN  DEVIATION  -   0.0031246    ROOT MEAN SQUARE  DEVIATION
                           [MODELS]      RESIDUAL SUM  OF SQUARES = 0.62780E-06
                                          MEAN  PERCENT  DEVIATION  =  17.6211090
                                                                                                                      0.0001379
                                          MEAN  DEVIATION =   0.0031848    RIJUT  MEAN SQUARE DEVIATION
                           [MODEL C]       RESIDUAL SUM  OF SQUARES » -0.15190E-05
                                          MEAN  PERCENT  DEVIATION =  25.8319580
                                                                                                                      0.0002145

-------
                  EOT 3UMS3 » lltO-G
                                              23 71
       ~XiI),GMS H2S04/BH C    RATE, GMS M2S04/GN C-KIN
           [MODEL'A]
CALCULATED RATE. CMS H2S04/G.M C-KIN
           [MODEL B]

CALCULATED RATE, CMS M2S04/GH C-MN
            [MODEL C ]

CALCULATED RATE, CMS H2SO*/GM C-HIN
O
U>
0.00292
0.00437
0.00583
0.00729
0.00875
0.01C21
0.01167
0.01312
O.C1458
O.OU23
0.02187
0.02552
0.02916
0.03281
0.03645
0.04010
0.04375
0.04739
0.05104
0.05468
0.05633 :
0.06197
0.06562
0.06926
0.07291
0.08020 -
0.08749
0.09478
0.10207
0.10936
0.11666
'- . , 0.12395
0.13124
0.13B53
0.14582
0.16040
0.17498
0.004S&33
0.0032855
0.0015552
0.0012923
0.0011317
0. 0010258
0.0009638
0.0009163
0.0008907
: 0.0003431
0.0008250
0.0003141
O.OOOB031
0.0007922
V ; 0.0007849
0.0007776
0.0007703
0.0007630
0.0007557
0.0007520 ' 	 '
0.0007447
0.0007374
0.0007333
0.0007265
0.0007228
: . . 0.0007119
.. .!...'".. 0.0006972
• 0.0006899
0.0006827
0.0006717
0.0006608
0.0006461
0.0006352
0.00062C6
0.0006097
0.0005804
0.0005513 '
0.0001753
., ..^. ..;,.. 0.0009716
... ' >r'r ."•;,=•"'• 0.0009678 . <•
.,--::.: . 0.0009640
0.0009603
0.0009565
0.0009527
:' - .'.' ':•;:',-'•';. '-: 0.0009489
::. -••:. "-. O.OOO9452
•-": "- .;" ->••'.;:'.•' 0.0009357 „
0.0009263
0.0009169
0.0009075
: \ .; .- . 0.0008980
"Cx -'."-.:;•.' J'- , 0.0008886
"'•'.. .';•':• •". ••••.•- 0.0008792
O.O008697
0.0008603
0.0008509
* 0.0008414
0.0008320
0.0008226
0.0008132
0.0008037
0.0007943
	 0.0007754
0.0007566
0.0007377
0.0007189
0.0007000
0.0006811
•!.'"• ,'vi ,,..;.. . 0.0006623 .-.:,>.
'"-.-' ••.-• "-V •'••'i''- . 0.0006434 '•'•
•• • ••>••.-. 0.0006246 ••••'
0.0006057
0.0005680
0.0005303
0.0011198
" ' ' 0.0011155 . . • ;
< ' ' x . 0.0011112 ' -.'.:;".. •
0.0011069
0.0011025
0.0010982
O.O010939
' , ' 0.0010895 - 	
o.ooioe52 '•'.. :
O.OO10744
0.0010635
0.0010527
•0.0010419
0.00103H ,:.;.-. ... • ,: •„
'•'•••' • 0.0010202 :!: '.'f.: ':. . • > - '.;
, , 0.0010094
0.0009986
0.0009878
0.0009769
'"•"" -,""' 0.0009661 '
< O. 0009553
, . 0.0009445 ' ,
0.0009336
0.0009228
0.0009120
, 0.0008903
0.0008687 '
< . 0.0008470 j.s-i
0.0008254
0.0008037
0.0007821
<•"- - ??:. ;'• •'**>!,•' 'IK**-.' • O.O007604 • '» '' •• v
:'v- •:,'•;'•; v '"V- ;;1".-" ', j • ' 0.0007388 ' ' •.•
•., .,"' 
-------
                  R'JH NUMBER • lUl-0
                U 26 71
o
-p-
               H2S04/GM c
RATEt'GMS H2S04/GM C-M1N
           {MODEL A]

CALCULATED RATE, CMS H2S04/GK C-MIN
           [MDDEL 3]

CALCULATED RATE. CHS H2SC4/GH C-KIN
           [MODEL C]

CALCULATED RATE, CMS M2S04/GN C-HIN
0.00146
O.C0296
0.00444
0.00592
0.00740
0.00888
0.01036
0.01184
0.01332
0.01480
0.01650
0.02220
0.02590
0.02960
0.03330
0.03700
0.04071
0.04441
0. 04611
0.05181
0.05551
0.05921 .:• :
0.06291
O. 06661
0.07031
0.07401 •"
C. 08141 *
o.cesei
O.C9621
0.10361
0.11101
0.11842 . > ... -
-. ' 0.12582 ." ' '
0.13322
0.14062
0.14802
0.16282
0.17762
0. 192*3
0. 0051181.
0.0042197
0.0023197
0.0011415
0.0009353
O.OOOD359
0.0007843
0.0007511
0.0007364
0.0007253
0.0007217
0.0007106
0.0007032
O.OC06959
0.0006849
0.0006775
O.U006702
0.0006628
0.0006554
O.OG064tiO
0.0006443
0.0006407
0.0006333
O. 0006260
0.0006223
0.0006149
0.0006038
0.0005928
0.0005818
0.0005671
0.0005523
•:•-• 0.0005339
1 C. 0005192 '
0.0005008
0.0004823
0.0004640
0.0004234
0.0003866
0.00
O.OOO7981
. - ., ;. • •••(•• 0.0007950. •••:•• •••••'.
.:i ' ''^::':;' ;VX:.; 0.0007919. v,'";;.>^.--.
••-••-•-•• 0.0007883 v
O.O007856
0.0007825
0.0007794
0.0007763
'-•'•;.. O.OC07732
• 0.0007700
0.0007622
0.0007544
0.0007466
. ,..;, : 0. 0007388
0.0007310
- :- '."••• 0.0007232 - - -
0.0007154
0.0007076
0.0006998
"'•' , . • 0.0006920
: -••'. . O.OOC6842 •• :• .•: :•
'.',">:'••.*• •: .: ~ <>.s .., . 0.0006764 '.-.-' •'."•'.
0.0006686
0.0006608
0.0006530
0.0006452 •;.•:?•,< '-. '•'••:
0.0006296 .'"••: '.V ?.'.
0.0006140 ' : . •".
0.0005984
0.0005828
0.0005672
- V "•« '!•:•' C" ••• 0.0005516
.••-.• ' ; •'/; 'I ; :": 0.0005360
: -.•;• •"' " 0.0005203
0.0005O47
0.0004891
0.0004579
- . 0.0004267 . • .
• •' ••.;'.• -'-A.: 0.0003955.' *.V "':
0.0008797
i .• • : .: . O.OOOS762
«.Jt; ,-:-.;• .„ .-v:;-'.;: ., ,~ o.ooos728
' ...• *.»:•::. ...' • O.OOOB694
O.OOOS659
0.0006625
O.C008590
0.0008556
0.0008522
0.0008487
O.U00640I
O.O008315
0.0008229
0.0006143
. ,-, O.C008057
0.0007971
O.CU07B35
0.0007799
0.0007713
- ~ :'- ;;•<:.?-•;. .. c.0007627
: :•::•••• .!.": •'" 0.0007541
'':•';'•,; '"\ -x ">•'.-'•; ; .. 0.0007455
0.0007369
0.0007283
0.0007197
.:; J-;v;:-'' yfyit^'Kfi'::,, 0.0007111
••••-;-,' • -:•. •'•:.' ; ^^^Ki^:5.<:.^^:V 0.0006939
,•':•''•* •' fc^vST-'.lAii: ' 0.0006767
0.0006595
0.0006423
0.0006251
" ; 0.0006079
*, - O.O005907
0.0005735
0.0005563
0.0005391
0.0005047
•.<.:., •..-.-.• ., • 0.0004703
•::. "••': ,*,:,'::> ...|-;"..- ,. 0.0004359
0.0010536
0.0010461
0.00103S6
0.0010311
0.0010236
0.0010162
O.OC10038
0.0010014
0.0009941
0.0009067
O.OOO9685
0.0009504
0.0009325
. O.OO09148
'• 0.0008972
0.0008797
0.0008624
0.0008453
' O.OOOU2U3
• 0.0008115
0.000794B
0.0007783
0.0007620
O.OO07458
0.0007297
•. , 0.0007139
:. ' 0.0006826
0.0006519
0.0006219
0.0005926
0.0005639
•';•"'• : 0.0005358
>"•'•:*'-. ':-• >"' . 0.0005084
:. i ••::. ...; : •. 0.0004316 	 _
0.0004555
0.0004301
0.0003812
•• •-•••;. ••-, ••-• • •:."' • 0.0003350
'•"'.' •'••' ' ..•:' ; : : •'-'•- 0.0002915 ':•'
                                                     MEAN DEVIATION =    0.0000328   ROOT  MEAN SQUARE DEVIATION
                                        [MODEL A]      RESIDUAL SUM OF SQUARES = 0.40Z35E-07
                                                     MEAN PERCENT DEVIATION -   5.5525742
                                                                                         0.0000349
                                                  "MEAN DEVIATION  =    0.0000982   ROOT  MEAN SQUARE DEVIATION
                                       [MODEL B]      RESIDUAL SUM OF SQUARES = 0.32985E-06
                                                     MEAN PERCENT DEVIATION =  16.2963409
                                                                                          0.0001000
                                                     MEAN DEVIATION  =    O.OOC1283    ROOT MEAN SQUARE DEVIATION
                                        [MODEL C]      RESIDUAL SUM  OF SQUARES * 0.7V487E-06
                                                     MEAN PERCENT  DEVIATION =  19.5493622
                                                                                          0.0001552

-------
            RU3 NUMBER
                                        U 27 71
XIII.CMS HZSO*/CM C     HATEt CMS H2SO*/G« C-HIN
       0.001*".
       O.OC2S8
       0.07431
       0.0057'i
       0.00719
       0.00843
       C. 01004
       C. 01150
       O.Cl*38
       0.01797
       0.02156
       0.02516
       0.02575
       0.03235
       0.0359*
       0.03953
       0.0*313
       0.0*672
       0.05012
       0.05191
       0.05750
       0.061 10
       0.06*69
       0.06829
       o.oTiae
       0.07907
       0.08626
       0.093*4
       0. 10063
       0.10792
       U. 11501
       0.12220
       0.12V38
       0.13657
       0.14376
       0.15814
       0.17251
0.0050370
0.003*817
0.0021380
O.OOP9639
0.0008334
0.0007573
0.0007067
0-OC06740
O.OCQS559
0.0006522
0.0006*1*
0.00063*1
0.0006233
0.0006160
0.00060b8
0.0006016
0.00059*3
0.0005870
O.C0057V8
O.CU05762
0.0005689
0.0005617
0.0005561
0.0005508
0.0005*36
0.0005*00
0.0005290
0.00051S2
0.0005073
0.0004965
0.000*655
0.000*7*7
0.000*638
0.0004*93
O.OU043*9
0.0004204
0.000391*
0.0003623
             [MODEL A]

 CALCULATED RATE. CMS H2S04/GM  C-MIN

            0.000678T
            0.0006761
            0.0006735
 _.    .    0.0006710
            0.0006684
            0.0006658
 	   0.0006632   _
            0.0006607
            0.0006501
  _     _   0.0006555
          ~ O.OC06'.91
            0.0006426
	    __   O.OO0636Z
            C.OC06297
            0.0006233
            0.0006168
            O.OCQ610*
            0.0006040
            0.0005975
 "	    • 0.0005911
            0.0005046
            0.00057B2
            0.0005717
            0.0005653
            0.0005509
            O.OOC5524
            0.000539S
            0.0005266
            0.0005138
            0.0005009
            0.0004880
            0.0004751
            0.0004622
_.	 ..  . 0.0004493
            0.0004364
            0.0004235
        	  0.0003978
            0.0003720
                                                                     [K032L B]

                                                        CALCULATEO~~RATEt GMS  H2S04/OM C-MIN
             [MODEL C]

CALCULATED RATE.  CMS H2S04/GM C-MIN
0.00072*2
- ••••'.:*:. 0.000721*
:•: . : • : 0.0007187
:•', :. • . • 0.0007159
0.0007132
0.000710*
0.0007077
0.00070*9
0.0007022
L-** ~ 0.0006994 . •
0.0006926
0.0006857
0.0006788
;:A- : •: . :>-:.:. 0.0006719
•;"j:- •"> ::'i 0.0036651 -'"•'"
"•\: : ': ••• O.noa65B2
O.C006513
0.0006*44
O.C006376
0.0006307
0.0006238
O. 0006169
0.0006101
0.0006032
6.0005963
O.OOC589*
0.0005757
0.0005619 :.-.
O.OC05482
0.00053*4
0.0005707
. 0.0005069
0.000*932
0.0004794
0.000*657
0.000*519
0.000*24*
0.0003969
o.oooasoo
0.00084*1
. O.OOOU383 :•
0.0008324 	
0.0008265
0.0008207
0.0008149
0.00011091
:. . • - 0.000803*
. ' . : 0.0007976
0.0007833
0.0007692
0.0007551
V-;; ,,;• ,.-. ,-, .i ; 0.0007*12
••- . •"':::'•' •".• 0.0007273
:. '• •.••••"•. , f 0.0007136
0.0007001
0.0006866
0.0006733
,,- ::,;,% ; 0.0006600 . •
ii.s.,. •;.•••?•••.... 0.0006*69 -'-'•''
• '.. 0.00063J9 .
0.0006211 "'
0.0006083
0.0005957
f •••>-. '^., •:,• V :-,'•.• -0.0005832 ,-• '. . '
•:••'••• •-. ,.' • 0.0005585 ' .
•-..-'?• .. :i,:;;^-y:< :-? 0.00053*3 ••' ' '• .•
0.0005107
0.000*875
0.00046*8
•v • - •' •• '''• 0.000**25 -'
>;V .''•"/. '•;<..• 10.000*208 " , ,
-• • 0.0003996
0.0003789
0.0003587
0.0003197
• . ,i. 0.0002828
                                                 MEAN DEVIATION  =    0.0000107    ROOT MEAN  SQUARE  DEVIATION
                                    I MODEL A]     RESIDUAL SUM OF SQUARES  = 0.579355-08
                                                 MEAN PERCENT DEVIATION »   1.8738451
                                                                                         0.0000135
                                                 MEAN DEVIATION  «    0.0000444    ROOT MEAN  SQUARE  DEVIATION
                                    [MODEL B]     RESIDUAL SUM OF SQUARES  - 0.68234E-07
                                                 WEAN PERCENT DEVIATION "   8.1341553
                                                                                         0.0000462
                                                 MEAN  DEVIATION -   0.0000788    ROOT MEAN SQUARE  DEVIATION
                                    [MODEL C]     RESIDUAL SUM  OF SQUARES  « 0.25634E-06
                                                 MEAN  PERCENT  DEVIATION «  13.9007187
                                                                                         0.0000895

-------
             SKI TOXBEH - 1U3-C
            U 28 71
XII I.CMS H2S04/GX  C    RATEt GM$ H2S04/CM-C-MIN
       0.0014*
       O.OC293
       0.00*35
       o.ooseo
       0.0072*
       0.008IS9
       0.01014
       0.01159
       0.01304
       0.0144*
       O.OIB11
       0.02173
       0.02536
       0.02898
       0.03260
       0.03622
       0.03985
       0.04347
       O.U4709
       C.C5071
       0.05434
       C.05796
       0.06159
       0.06520
       0.06883
       0.07245
       0.07969
       O.08694
       0.09418
       0.1C143
       0.10867
       0.11592
       O.12316
       0.1J041
       0.13765
       0.14490
       0.15939
 0.00336B3
 0.0021586
 O.OOIC10J
 0.0008330
 O.C006990
 0.0005157
 0.0005577
 O.CC05216
 O.CC.G4962
 O.OC04BIT
 0.0004745
 O.C0046J6
 0.0004564
 0.0004527
 0.0004455
 0.00043B2
 0.0004346
 O.C/004310
 0.0004238
 O.OC04201
 0.0004165
 0.000*129
 0.0004093
 O.O004056.
 0.0004020
 0.0(103964
 0.0003943
 0.0001B75
 0.0003B03
 0.0003730
 O.OOC36SB_
 0.00035S6
 0.0003477
 0.0003404
 0.0003332
0.0003223
0.0003006
                                 [MODEL A]

                    CALCULATED RATE, CMS H2S04/GM C-MIN
 0.000514J
 0.0005124
 0.0005104
 0.0005084
 0.0005065
 0.0005045
 0.0005025
"O.OC05006
 0.00049B6
 0.0004966
"0.0004917
 O.C004R68
 0.0004019
 0.0004769
 0.0004720
 0.0004671
 0.0004622
 0.0004573
 0.0004523
 0.0004474
 O.C004425
 0.0004376
 0.0004326
 0.0004277
 0.0004228
 0.0004179
 O.OC04080
 0.0003982
 0.0003833
 0.0003765
 0.0003687
 0.0003588
 0.0003490
 0.0003391
 0.0003293
 0.0003194
 0.0002997
                                       {MODEL B]

                          CALCULATED  RATE. CMS H2S04/SH C-MIN
            [MODEL C)

CALCULATED  RATE, CMS HZS04/CK C-KIN
0.0005192
,'": .,: ,.. ;.. 0.0005172
; ' 0.0005152
'.-•••:'. :. 0.0005132
0.0005113
0.0005093
0.0005073
0.0005053
* - - '- . 0.0005033
0.0005013
O. 0004963
0.0004914
0.0004B64
0.0004814
,-' 7' ' 0.0004765
. - ~ C.OC04715
0.0004665
O.C004616
O.O004566
..v-f.) ... s- , 0.0004514 , '
::";,v*- -".. 0.0004467
:.:< i ;:,: 0.0004417
0.0004367
0. 0004318
0.0004268
O.OOC4218
0.0004119 :, .: : ."..'.
0.0004019 '•''•'
0.0003920
0.0003821
0.0003721
'" 	 "' 	 0.0003622 .\/ ;,.:,- .
O.OOO3523 ' : - ' ~
0.0003423
0.0003324
0.0003225
0.0003026
0.0005887
0.0005845
O.O005004
0.0005763
0.0005723
0.0005682
0.0005642
0.0005601
0.0005561
0.0005521
0.0005421
0.0005322
-0.0005224
0.0005127
0.0005030
.: 0.0004935
0.0004840
0.0004746
0.0004653
'• . •.:•: 0.0004561
•:.; 0.0004470
, J .. \-~ -:'• 0.0004379
0.0004289
0.0004200
0.0004112
-X ' ••.-;.-:•. '!.-•,.•••:... O.OCC4025 •-
'•• .-.•..; .' : •: O.C003685 • •
0.0003520
0.0003358
0.0003200
• . ,. - ; •;'"-. ' ... . 0.0003046
' "• ' •'- • -•••:- - - 0.0002894
•". ,:.-.. „'. ,.;: 0.0002747
0.0002603
0.0002462
0.0002191
                                                MEAN DEVIATIOM  =    0.0000173    ROOT MEAN SQUARE  DEVIATION
                                  [MODEL A]      RESIDUAL SUM OF SQUARES  = 0.13874U-07
                                                MEAN PERCENT DEVIATION -   3.9458380
                                                                                         0.0000212
                                                MEAN  DEVIATION  =   0.0000202    ROOT MEAN SQUARE  DEVIATION
                                  [MODELS]   '   RESIDUAL SUM OF SQUARES  = 0.174A8E-07
                                             '   MEAN  PERCENT DEVIATION =   4.6428303
                                                                                         0.0000237
                                                MEAN  DEVIATION =   0.0000443    ROOT MEAN SQUARE  DEVIATION
                                  [MODEL C]     RESIDUAL SUM  OF SQUARES = 0.76i88C-O7
                                                KEAN  PERCENT  DEVIATION  =  11.0762110
                                                                                         0.0000496

-------
           E'JTf SVMEER • liU-G
                                       29 71
XIDtCKS H2S04/GH C
                     KATE, CHS H2SC*/GM C-MIN
           [MODELS]

CALCULATED RATE, GMS H2SO4/SM C-MIN
            [MODEL B]

CALCULATED RATE, CHS H2S04/GM C-MIN
            [KOBE! C]

CALCULATED RATE,  CMS HZSOWGM C-MIN
0.00213
O.CO**0
0.00596
0.00713
0.00830
0.01026
0.01173
0.01330
0.01*46
0.01833
0.02199
0.02566
0.029J2
O.C32TJ
0.03645
0.0*032
0.0*3*9
O.C*7i5
0.05132
0.05*98
O.C58S5
. 0.06231
0.0.6598
0.0696*
0.07331
1 o.caoi*
0.08797
O.C9530
0.10263
0.1C936
0.11730
"! ' .' 0.12*63
0.13196
•:" 0.13929
0.1*662
0.16128
0.1759*
0.19061
0.20527
0.0053*89
0.0037517
0.0025251
0.0015452
C. 001*26*
0.0013559
0.0013001
0.0012518
0.0012035
0.0011367
0.0010995
0.0010810
0.0010698
0.0010623
0.00105*9
0.0010*7*
0..0010'.00
0.0010326
0.0010252
0.0010215
0.0010178
0.00101*1
0.0010066
0.0010030
0.0009992
0.0009918
; '. 0.00098*3
. 0.0009769
0.0009658
0.0009509
0.0009398
0.0009212
0.0008989
' O.OOOB766
0.00005**
0.0008060
0.0007577 •
0.0007058
0.0006538
0.0012691
0.00126*1 " '
0.0012592
" 0.00125*3
0.0012*93
0.0012***
0.0012395
0.00123*5
0.0012296
0.0012173
0.00120*9
0.0011926
0.0011803
0.0011679
0.0011556 " .".-*,
0.0011*32
0.0011309
0.0011186
0.0011062
0.0010939 •.>"%.'- <•>'.-. • •• JS<,v. ;.' ••• ..;••
0.0010816 •:•-•"": ,',,.. ••" " ••v":- <••••
0.0010692 •• "•-•••• ' ' ' • •" • :-'f'''i' '•'••'• "-'
0.0010569
O.O010**5
0.0010322
'". 	 """ 	 o. 0010075- •C:^.V:.-:;;T;";:U:;-; S^;;:':'?^'1
0.0009829 v:^;;" !'.- ' .'' .i "' f$":r- -'••
0.0009582 • • ••• • ••'• :-.. •• •• :•;••-:•. .: . ,
0.0009335
0.00090S8
0.00088*2
. :•'.';,';"-,• ' ;;,..?:.•.?! vV*'S."';.k 0.0003595 'V^ " ;••;' >;':.- • 	 „"
'•'*•*••':• ••-.;-•'••*.• '."•'•' 0.00083*8 ':'r '' '-' : • • •• •
•"'• ' '< . :i i l: o.oooeioi ..:.;!.. :•
0.0007855
0.0007361
0.0006868
• .•• ":'..:Y- ::-.i: 0.000637* •: ,~ ,y\r. - :'•.-• -"*..:., ••>.,.••:•
•-. . . •:--. .-. . • • ;;-• •:-.. 0.0005881 -.:.:., v.:. >••/: ^ - •<'•• «-:'-\?* •• i...;>-
0.001*233
0.001*178 : -
0.001*123 ;V
0.001*067
0.001*012
0.0013957
0.0013901
0.00138*6 -.
0.0013791 ">;•'" '"'"'
0.0013652
0.001351*
0.0013375
0.0013237
O.OOU099
0.0012960
0.0012822 •
0.001268*
0.00125*5
0.0012*07
0.0012269 ••:-•:• : .•„ '
: 0.0012130
0.0011992 •!..
0.001185.3
0.0011715
O.OOU577
O.OOU300 '•'•'' '; • ;--'V •;:>•
0.0011023 : ":M:. •,- •';.••
: . 0.00107*7 >•;'•' • .'• '
0.0010*70
0.0010193
0.0009916
0.00096*0 .».--.
0.0009363 ' ''•
0.0009086
0.0008809
0.0008256
0.0007703
0.00071*9 , : .
?,;. 0.0006596 . ' ":.',•••• •'/..
0.0017239
0.0017117
0.001699S
0.0016873
0.0016752
0.0016631
0.0016510
0.0016390
0.0016271
0.0015973
0.0015678
0.0015386
0.0015096
0.001*808
0.001*523
'.••••• 0.001*2*1
0.0013961
0.0013683
0.0013*08
- '•• •-:,:.. '•,!..... . s 0.0013136
0.0012866
: ' :•;•: 0.0012599
0.001233*
0.0012072
0.0011812
. ';. :;.••...;•• ,.,;. ; . O.OOU301
;. •.;••..•.,*, ,::;.;•;.• 0.0010799
• .;::.>:^;.. :. '•' 0.0010308
0.0009828
0.0009358
0.0008898
i..:.i .::• *'•:•', o.oooe**9
: •••••: ' • .- o.oooaoio
•.. ,:;;.. 	 •'•;.; .-.• 0.0007592
0.0007165
0.0006363
0.000560*
• ; ; ,-•- 0.0004889
V.'j'-;/'.>-viv.«i- 0.000*219 ••••'• •
                                              MEAN  DEVIATION =    0.0090647   ROOT MEAN  SUUARE DEVIATION
                                 [MODEL A]     RESIDUAL SUM Of SQUARES « 0.17218E-06
                                              MEAN  PERCENT DEVIATION  *   fa.5631943
                                                                  0.0000712
                                              F.EAN DEVIATION -    0.0001368'  ROOT MEAN  SQUARE DEVIATION
                                 [MODEL B]     RESIDUAL SUM OF SQUARES * 0;8886lE-06
                                              MEAN PERCENT DEVIATION «  13.0999966
                                                                  0.0001617
                                 [MODEL C]
  MEAN DEVIATION  »    0.0002509   ROOT  MEAN SQUARE DEVIATION
  RESIDUAL SUM OF SQUARES = 0.27905E-05
  Hf-AN PERCENT DEVIATION =  2
-------
                  ROT KUMBEB « 1U5-C
U 30 71
       XII),GHS HZS04/GN C    RATE, GHS H2S04/GH C-HIN
                   [MODELS]

        CALCULATED RATE, GHS H2304/SM C-HIN
           [MODEL B]
CALCULATED RATE, CMS H2S04/GH C-HIN
            [MODEL C].

CALCULATED RATE, GHS H2SO4/6H C-HIN
O
CO
0.00290
0.00436
0.00531
0.00726
0.00871
o.oioir
0.01162
0.01307
O.C1452
0.01915
0.02178
0.025*1
0.02904
0.03267
0.03630
0.03994
0.04357
0.04720 .
0.05093
' . 0. 05446
One ano
O.C6172
0.04535
0.06698
0.07261
"" 0.07987
0.08713
0.09429
0.10165
0.10391
0.11618
0.12344 -
'•' 0.13070 '
0.13796
0.14522
0.15974
0.17426
0.0064766
0.0051453
0.0037780
0.0026626
0.0014752
0.0010650
0.0010218
0.0009931
0.0009715
O.C009319
O.COC0031
0.0003616
O.OC08635
0.0008455
0.0008312
O.OOOP203
O.OCOB096
0.0007988
O.OOO7916
0.0007644
OPOfl 1777
0.0007700
0.0007628
O.O007556
0.000752C
0.0007412
0.0007268
. '.. : 0.0007124
0.0006980
0.0006764
0.0006621
0.0006405
0.0006225
0.0006009
0.0005793
0.0005362
0.0004893
0.0008921
-.-•; .'••.•>:..• 0.0008887 ' - *
:, '-"',\\:. ";;';.•.•; ,'.o.oooas52 "" ' ^
' " .'•"••'•'' 0.0008818 < ..
0.0008783
0.0008749
0.0008715
> ,,J c - - 0.0008680 *'•*
0.0008646
; '• * - ' - 0.0008560
0.0008474
0.0008388
0.0008302
0.0008217
0.0008131 f
0.0008045
0.0007959
0.0007873
0.0007787
, V ;. „ . : . 0.0007701
-•••-.• .--•••-• '- -,-:' ' •' A non7&is
. •'. '•. •'''. *;: '"'/' ..;. : 0.0007530 .
0.0007444
0.0007358
0.0007272
'" ' 	 0.0007100 	 ' "
0.0006928
0.0006757 	 .._. 	
0.0006585
0.0006413
0.0006241
, ,, 0.0006069 - - • •
" "' ' ,' 0.0005898 . ' -v, , ,
0.0005726 . 	 ' 	 ,
0.0005554
0.0005211
0.0004867
0.0010061
0.0010023
O.OOC9984
0.0009945
0.0009906
0.0009868
0.0009829
O.C009790
0.0009751
__ 0.0009654 ^1 : • '.' ... . .
0.0009558
0.0009461
0.0009364
0.0009267
0.0009170 '
0.0009073 •••.'• • '
O.OOOS976
o.oooaa»o
0.0008783
0.0008686 • . • . ;•-•• . •; • • .,.
OOOC8589 •" " ""
0.0008492 '^i'--. ••• ' ;•>•? i--
0.0008395
O.O008298
O.C008201
0.0008008 .r.,-,. .:. . : - .
0.0007814 •?.-'••/ ~:'^- ' . 'f--- -i •:"'•'
0.0007620 '•' 'I--. '"',-• ,.". '' .'• •' -
0.0007427
0.0007233
0.0007039
• 0.0006845 .-'-. '•:•-•: •" : • 'V. , '/. '
0.0006652 ••• •• • '•• •'•
0.0006458 . ' ' £":" ' '
0.0006264
0.0005877
0.0005489
0.0012187
0.0012101
0.0012016
0.0011930
O.OC11846
0.0011761
0.0011677
O.C011592
0.0011509
0.00113CO
0.0011094
0.0010869
0.0010686
0.0010484
0. 0010265
O.OC10037
0. 0009890
0.0009696
0.0009503
0.0009312
0 .C 009 123
0.0008936
O.OC087SO
0.0008566
0.0008384
• O.OOOS025
0.0007674
0.0007329
O.OG06992
0.0006661
0.0006339
0.0006023
0.0005715
0.0005414
0.0005120
0.0004556
O.OOC4021
                                        [MODEL A]
         MEAN DEVIATION =   O.O0004I8    ROOT MEAN SQUARE  DEVIATION
         RESIDUAL SUM  OF SQUARES » 0.11267E-06 '
         MEAN PERCENT  DEVIATION »   4.9554777
                                                                                                                       0.0000594
                                                      MEAN DEVIATION  =    O.CC00602   ROOT  MEAN SQUARE DEVIATION
                                        [MODEL B]       RESIDUAL SUM OF SQUARES = 0.13U6E-06              ... ......
                                                      MEAN PERCENT DEVIATION -   7.9813900
                                                                                                                       0.0000640
                                                      MEAN DEVIATION  =   0.0001177    ROOT  KEAN SQUARE DEVIATION
                                        [MODEL C]       RESIDUAL SUM  OF SQUARES = 0.58060E-06
                                                      MEAN PERCENT  DEVIATION =  14.6390228
                                                                                                                       0.0001347

-------
           HOT HUMEH « 1U8-G
                                     5  7 71
                                                         [MODEL A]
[MODEL B]
XCD.GHS H2S04/GM C    RATE, CMS H2S04/GM C-KIN  CALCULATED RATE, CMS H2S04/C1 C-MIN  CALCULATED RATE, CMS H2S04/GK C-H1N
             [MODEL C]

CALCULATED RATE,  GHS HZS04/CH C-HIN
C. 00229
0.003*3
0.00*57
0.00572
0.00686
0.00801
0.00915
0.01029
0. 01141.
	 0.01429
0.01715
0.02031
0.02237
' 0.02573
0.02659
0.031*5
0.03*31
0.03717
0.0*003
0.0*238
0.0*57*
0.0*860
0.051*6
0.05*32
0.05718
O.C6290 ...,../
0.06862 . '
0.07*33
O.CS005
0.06577
0.091*9
7 o.o972i ; •
0.10232 : ,
0.10364 ...-•.-
0. 11*36
0.12530
0.13723
•0.1*867 ' '
0.16010
: 0.1715*
0. 16298
0.19*41
0.20535
0.21728
0.0216960
0.0199966
0.018*388
0.017051)9
0.0157197
0.01*473*
0.0133122
0-0122359
0. 0112162
O.OC87520
O.O067127
0.0051Z66
0.00*1636
0.0038010
0.0035:22
O.OOJ2573
0.0030307
O.C02S3Z4
0.0026908
0.0025718
0.002*755
0.00238*9
0.0022999
0.0022262
0.00215D3
0.0020337
0.0019090 .
0.0017957
0.0016936
0.001597*
0.0015068
0.001*218
0.0013312
0.0012*57
0.0011669
0.0010196
0.000889* '
0.0007760
0.0006798
0.00059*8
0.0005155
0.000*362
0.0003682
0.0003059
0.0019391
V'«..;:.- ^ •-• - 0.0019333
'. ..•-*.".:: -"".. 0.0019274 '
', • • -: 0.0019215. . ,
0.0019156
0.0019093
0.0019039
0.0018980 -. .; , :>•
.• .' .,,',••.' - 0.0018922 '..':.-•'" '';-,-'. • : '
• 0.0018775 . " '
0.0018628
0.0018*81
0.0018335
, . -,,;. . •-...! 0.0018188 <
..' -; >; f,' : 0.00180*1
0.001789*
0.00177*7
0.0017601
0.0017*54
0.0017307
0.0017160 s
, * " 0.0017014
0.0016867
0.0016720
0.0016573
0.0016280
0.0015986
0.0015693 * -<
0.0015399
0.0015105
0.001*812
• •'•:•.••• •-'•'-'• 0.0014518 •;•• :- ", ' •':•..• : '.• -.
".".x.C'' •,"%<- '•.:>': . 0.001*225 ' >''•*•..*« f .'i- '•..%* - '••-•''>'''' .<;''
: .... . •-• -;x: . <;- .•:*...;. 0.0013931 :•;•„•,•-... -.-v^. ... ....
0.0013638
0.0013051
0.0012*63
. .. '-:•:. •-,... 0.0011876 :;, -••••'•.-. :>
" •' <':•-,. :Ai?j..;.;. - O.OOH289 l's.,\ '-.-. .r.;: '• :. •:•... ,:• :f: -,:,-
:'-• •• •: "••'• 0.0010702 •••••-•< •• • .. : .. •;,...
0.0010115
0.0009528
0.00089*1
; ....;.. 0.0008354 ' .
0.0021979
0.0021912
0.00218*5
0.0021779
0.0021712
0.00216*6
0.0021579
0.0021513
O.OC21**6
0.00212bO
0.0021113
0.00209*7
0.0020731
0.0020614
C..00?0**8
0.0020282
O.OC20115
0.00199*9
•O.OC19783
.. 0.0019616
0.0019*50
O.C019284
0.0019117
0.0018951
0.0018784
O.OOl8<-52
0.001B119
O.OD177S6
0.0017*5*
0.0017121
0.0016788
0.0016*55
0.0016123
0.0015790
0.0015*57
0.001*792
0.001*126
Q.0013'61
0.0012795 .:
'••• 0.0012130
0.0011*65
0.001C799
0.0010134
0.0009468
0.002«03i
0.0027881
. 0.0027726
0.0027572
0.0027413
0.0027264
0.0027111
0.002695B
0.0026806
	 0.0026*27
0.0026050
0.0025675
0.002530S
.: : 0.002*934
0.0024567
0.002*202
0.00238*0
0.0023481
. 0.0023124
V '." 0.0022769
0.0022*17
• , •••' -A... 0.0022067
0.0021720
0.0021376
0.0021033
• •••-• • -"'."•''•;-;: •;.:. v; 0.0020357
..;.:.: ' •' 0.0019690
' . >'- ... > 0.0019033
0.001B387
0.0017750
0.001712*
;, -, ,. ".":;•• .•, .: . 0.. 0016508
. . " ":' :,. 0.0015903
: ' ... "".*• 0.0015307
0.001*722
0.0013583
0.0012*96
„ - ' .:; . O.OOU430
. .,..:. ;..'. •••••.':.: : . 0.0010418
•••• • • • •' '•• X . . 0.0009*48
0.0008521
0.0007638
0.0006798
, . •;.;. '.,' ; D. 0006004 ..
                                              MEAN DEVIATION  =    0.0014892   ROOT  MEAN SQUARE DEVIATION
                                [MODEL A]      RESIDUAL SUM OF SQUARES = 0.29836E-03
                                              MEAN PERCENT DEVIATION "  47.7Z67*56

                                              MEAN DEVIATION  «    O.OOJ4-132   ROOT  M(-A,M SQUARE DEVIATION
                                [MODELS]      RESIDUAL SUM OF SQUARES = 0.27639E-03
                                              MEAN PERCENT DEVIATION =-  51.2974701

                                              MEAN DEVIATION  =    0.00.'1621   RUOT  MCAN SCUARE DEVIATION
                                [KOI-EL C]      RESIDUAL SUM OF SQUARES * 0.23324S-03
                                              MEAN PCRCCNT DEVIATION =  33.4808197
                    0.0028397
                    0.0027331
                    0.0025108

-------
           RU3 NUMBER »  1U9-0
5 10 71
Xltl.CHS HZSO*/GK C    pATEt CMS H2SO*/GH C-MIN
                    [MODEL A]

        CALCULATED RATE, CMS H2S04/CM C-HIN
            [MODEL B]

CALCULATED RATEi GHS H2S04/GM C-MIN
             [MODEL C]

CALCULATED RATE. CHS H2SQ4/GH C-MIN
0.00569
0.00682
O.C0796
0.00910
0.01023
0.01137
0.01*21
0.01706
0.01990
0.0227*
0.02559
0.026*3
0.03127
0.03*12
0.03696
0.03930
0.0*26*
0.0*549
O. 0*633
O.C5H7
0.05*32
0.05686
0.06255
0.06623
0.07392
'< 0.07960
O.OB529
0.09093
0.09666
0.10235
0.10803
0.11372
0.12509
0.136*6
0.1*78*
0.15921
0.17058
0. 18195
0. 19332
0.20*70
0.0151080
0.0137051
0.012*101
0.0112231
0.0101979
0.0092536
0.0071223
0.005*766
O.OC".2356
0.0029137
0.0025B99
0.002196D
0.002023*
0.00190*1
0.0018211
O.OU17563
0.0017131
0.0016781
0.0016*30
0.0016106
0.0015703
0.0015162
0.0014569
0.001*029
0.0013516
0.0013058
0.0012518
O.OC11979
0.0011*39
0.0010872
0.0010279
O.OC09065
O.OC07878 ::
0.0006771
0.000577*
0.000*856 '
0.000*0*7
0.00033*5
0.0002779
0.0015665
<• .,..":. 0.0015618 ,-. ,,,:..,.
0.0015570 : '••
0.0015523
0.0015*75
0.0015*27
0.00153CB
0.00151E9
. • ••-.';•'' ••>••'• 0^0015071 •-•:.;••<:..::;•:-,:-:
0.001*952 '•'..'
0.001*833
0.001*71*
0.001*595
:, - : ••••• >. ' 0.001**76
" V;,7'.' '•'.' 0.001*357
-..! 0.001*238
0.001*119
0.001*000
• 0.0013801
.. . .„• v.. ; . 0.0013762
. : , . ;..;K:-/S" 0.00136*3
• ;- : •'•" 0.001352*
0.0013286
0.00130*8
0.0012810
	 o.ooi2572 ;r^: -:';••'; ".,' :
0.001233* '" ':-'V; '•',/-"•'-' •'• •
0.0012096
0.0011058
0.0011620
0.0011382
•:•<••_ ., ••, .; :..>.:• .•'. 0.00111** ,- ' •, .
~ -••--.. •:•••-•• 0.0010668 •-. : . . .
(,' •':-'••:••'.:' , o.ooioi92 :«•--:•>;;. :.-^L;
0.0009716
0.00092*0
0.000876*
'• '•••• '•;• 0.0008289 ' ' '
	 -',.-.- '-. . 0.0007813 • '•-.: -... .-
. :: •• : '•:'.. 0.0007337 t 	 - : ;
0.00170*5
<-.. ..." . •••:. •••!'••' 0.0016993
->•>• •:• ''' :.';?• 0.00169*1
' 0.00168B9
0.0016837
O. 0016786
0.0016656
:••:'•' • •'-;' ••• 0.0016S27
f > .-' ' ; 0.0016397
. ; ." 0.0016268
0.0016138
0.0016009
0.0015679
0.0015750
;, 0.0015621
O. 0015*91
O.CC15362
0.0015232
0.0015103
0.001*973
0.001*8**
0.001*71*
0.001**55
0.001*197
0.0013938
,. . ?\.f .;.:: •.:,'-.,.:.• 0:0013679 . -
:V> ; .-.-:;- -• .", 0.0013*20 . •.• ,
-,-.', ••:.'- '••• ''••- '.--' 0.0013161
O.OC129C2
0.00126*3
0.001238*
.•.v,:-.-.- :u.:' 0.0012125 . . .
->,;:•• ,;.\ .,.;<- 0.0011607 '''-
' ::„. .,:....-, :'. O.OOU090
0.0010572
0.001005*
0.0009536
0.0009018
. . ;. ..... 0.0000500
.. •;•-• •" .. 0.0007983
0.0021036
0.0020V19
0.0020802
0.0020570
O.OU2045S
O.OC2C167
O.OOIS3BI
0.0019'j97
0.0019315
0.001903*
O.OOIH756
0.0018*79
0.0018204
0.0017931
0. 0017660
0.0017391
0.001712*
. 0.0016859
0.0010595
0.001633*
••'":. 0.001607*
0.0015560
0.001505*
0.001*555
• • •- • 0.001*06*
'•••-•• 0.00135S1
. 0.0013105
0.0012637
0.0012177
0.0011724
. :- ' 0.0011280
.". 0.0010*1*
',"••'.' " 0.0009580
0.0008777
0.0008006
0.0007268
0.0006562
0.0005889
0.00052*9
                                [MODEL A]
        MEAN DEVIATION =    0.0011285   ROOT  MEAN SQUARE DEVIATION
        RESIDUAL SUM OF SQUARES « 0.19876E-03
        MEAN PERCENT DEVIATION =  39.9634857
                                                                                                                0.0023497
                                [MODEL B]
         SEAN DEVIATION  *   0.0010806    ROOT MEAN SQUARE  DEVIATION
         RESIDUAL SUM  OF SQUARES = 0.18962t-03
         MEAN PERCENT  DEVIATION) »  40.9921875
                                                                                                                0.0032951
                                [MODEL C]
         MEAN DEVIATION »   O.OC09072    ROOT MtAM SQUARE  DEVIATION
         RESIDUAL  SUM OF SQUARES =  0.16619E-03
         MCAN PFRCF.NT DEVIATION *   25.7657623
                                                                                                                0.0021485

-------
          R'JS rUMBES • 150 -G
                                     5 11 71
                                                         [MODEL A]
[MODEL B]
[MODEL C]
XdltGNS H2SO*/GM C    RATE,  CHS H2S04/GM C-MIN   CAtCUUATEO RATE, CHS H2SO*/6M C-H1N  CALCULATED RATE, CMS  HZSO+/GH C-HIN  CALCULATED RATE, CMS H2S04/GM C-H1N
0.00427
O.C5533
O.C0540
C.C0747
O.CI553
O.C0960
0.01C67
0.01333
0.01600
• 0.01867
O.C2133
0.02*00
0.02566
0.02933
0.03200
0.03^66
0.03733
o.o<-ooo
0.0*266
0.0*533
0.0*833
0.05266
0.05333
O.C5666
0.06400
O.C6933
O.C7466
0.07999
O.OS533
O.C9C66
0.09599
0.10133
C. 10666
0.11733
0.12799
0.13666
C. 1*932
- - - - 0.15999
0.17066
0.18132
0.0162019
0.01322*0 ' ' -.-
0.0112303
0.00956*7
0.009151*
0.0069*00
0.005905*
0.0039369 , , ,'i
0. OUZ6751 - ';•• ' •
0.0018675 '•''•"• 1
0.001*637
O.OC12113
0.0011180
0.0010*23
0.0010120
0.0009994
O.0&098*2
O.G009792
0.0009691
O.OC0959Q 	
0.0009*69
0.0009*13
0.0009312
0.0009110
0.000898*
O.OU08732 . 	
O.O008505 •
0.000(5303 - :
0.0008101
0.00078*9
0.0007621
0.0007*20 " - ' ' ;; .
0.0007167 ,V, •.•£•:".;'-;
0.0006663 . ;- ", • ....
0.0006157
0.0005552
0.000-'.9*6 '
0.000*189 . • ••
0.0003*07 ., . .. .:'.,
0.000262*
0.0010133
• •< • ' c. 001010* '•: "•.-.•.'•. V: .'•••:••,•- ;.~
0.0010075 •...'••;','.'•'• •"'•If •"-'..
. 0.00100*7 •".': ..... -.:'.:..< •'.,
0.0010018
0.0009989
0.0009. 0.0009385 ;". v ; .'•,-.;;•
'• 0.0009313 . -. , . .':<•-'•">
0.00092*1
0.0009169
'0.0009097
0.0009026
0.000895*
0.0008882
0.0008810
0.0008666
0.0003522
" ,. 0.0008378 :.. -: :.»; ..
0.0008235 ;-. • >'-; " '
0.0008091 ' . ' /',
0.00079*7
0.0007803
0.0007659
->' 0.0007515 : 	 : ;V .: ,
0.0007372 . ' •.••
, v . 0.000708* •' . .,-.
0.0006796
0.0006509
0.0006221
0.0005933 . ' > -: :•-, ...-•.;
'•":(•.• 0.00056*6 ;...;..;,-.,. •!•:„;: :.:-•••• f* 3 :-:-&
0.0005358 ' ' . :~ • .
0.001009T
0.0010069
0.00100*0
0.0010011
0.0009983
0.000995*
0.0009925
•;..-.'• 0.000985*
0 .0009782
: 0.0009711
0.0009639
0.0009557
0.0009*96
. 0.0009*2*
0.0009352
0.00092B1
0.0009209
0.0009137
0.0009066
0.000699* - '
0.0006922 • '•'•,'
0.0008051
0.0008779
O.C008636
0.2008*92
0.00083*9
0.0003206
0.0008062
0.0007919
0.0007776
0.0007632
0.0007*89 '.; •
0.00073*5
0.0007059
0.0006772
0.0006*86
O.OC06199
. '-: 0.0005913
:V V 0.0005626 • " I -:.;'
' : . O. 0005339
C. 0011833
0.0011771
0.0011710
0.00116*9
0.0011589
0.0011527
0.0011*67
0.0011316
0.0011165
0.0011016
0.0010868
0.0010720
0.001057*-
0.0010*28
O.OC102U*
0.00101*0
0.0009997
0.0009855
0.0009714
-. "• 0.000957*
. .:.«• ' 0.0009435
"-' : ' ' 0.0009297
0.0009160
O.OOOBSBS
0.0006620
O.OC08355
. , -• •••' '• 0.0008095
> - ....' . 0.0007838
0.0007585
0.0007336
O.OCC7090
•; , ..;.,... .. ... 0.00068*8
0.0006610
.: .: 0.00061*6
0.0005697
0.000526*
0.000*8*6
': 0.000***.*
. . - - 0.000*057
0.0003687
                                              MEAN DEVIATION «    0.0003888    ROOT  MEAN SQUARE DEVIATION
                                 [MODI, A]      RESIDUAL SUM  OF SQUARES - 0.37030E-04
                                              MEAN PERCENT  DEVIATION «  20.6231384
                    0.0010436
                                              MEAN DEVIATION =   0.0003903    ROOT MEAN SQUARE  DEVIATION
                                 [MODEL B]      RESIDUAL  SUM  OF SQUARES = 0.37110E-04
                                              MEAN PERCENT  DEVIATION =  20.6951752
                    0.0010447
                                              MEAN DEVIATION =   0.0003336    ROOT MFAN SQUARE  DEVIATION
                                 [MODEL C]      RESIDUAL  SUM OF SQUARES = 0. VU41 E-04
                                              MfcAN PERCENT DEVIATION  t  U.1673651
                    0.0009962

-------
                  RUT) KUMBEH - 151-0
                                             5 12 71
                                                                [MODEL A]
[MODEL B]
                                                                                                                                    [MODEL C]
        XU1.GHS MZSO*/GM C   RATE, CMS  H2SOVGM C-HIS   CALCULATED RATE. CMS H2S04/GK C-HIN CALCULATED RATE. CMS H2SOWGM C-HIN   CALCULATED RATE, CMS H2S04/SN C-f
t-0
0.00164
0.00327
0.00*91
0.00655
0.00819
O.OC982
0.0!l*6
0.01310
0.01*73
0.01637
0.020*6
0.02456
0.02265
0.0327*
0.0363*
0.0*093
0.0*502
0.0*912
0.05321
0.05730
0.06139
0.065*9
0.06958
0.07367
0.07777
0.08186
0.09005
0.09823
0.106*2
0.11*63
0.12279
0.13098
0.13916
0.1*73*
0.0028832
0.0020756
0.001*617
0.0010903
O.C009207
0.0008076
O.OOC7268
O.C006663
0.0006219
O.C035395
0.0005330
0.00050*7
0.000*8*5
0.000*765
O.OOO*68*
0.600*6**
0.000*60*
0.000*563
0.0'JO**83
O.COO***2
0.000*361
0.000*280
0.000*199
0.000*119
0.000*078
0.0003957
0.0003796
0.0003635
0.0003*72
0.0003311
0.0003109
0.0002908
0.0002665
0.0002*63
0.0003256
. :.-•,-.. :::,;.,„,•. 0.00032*2
. V,:;\ :•:• .. <•-•;: o. 0003229
•-••• : 0.000321*
0.0003200
0.0003186
0.0003172
•:- 0.0003157
''•' ' •' 0.00031*3
'."• 0.0003129
0.000309*
0.0003059
0.000302*
• . ; -'•'' ...:. ',-'.. 0.0002988
. -, ' •- -. •: • :•'.;' 0.0002953
" -:'v?i-> ..::.' 0.0002918
0.0002883
0.00028*7
0.0002812
' • 0.0002777 ...... • .'. ,.:.:i :
, ', 0.00027*2 . ;-'':lv V>.- ;' "- '•":• :.'"<*
, . . ' / - 0.0002707 . V-; •.:*• :; •- ' ':: '/ : '"'
0.0002671
0.0002636
0.0002601
v;*-V' ,.•.;•>.. ,-..•.:••: 0.0002566 " 	 "" ""
:'" :.' ::~-.',;s:*;;.^:..:.v: --0.0002*95
1 ' ' ••'•'• -•'.":- 0.0002*25
0.000235*
0.000228*
O.C002213
'-.••:•••• ;;,»;,v;:-..: 0.00021*3 • ; ',c -,.;•, '/• '•'.".';,."
; - : .;' -: 0.0002073 : ' -; • ": -- '•• ~
:, .-.'•' >..vO. 0002002 >Vi: ..-''• J ?,:"' •'..:'
0.0003817
0.0003BOO
0.000378*
0.0003767
0.0003751
0.000373*
0.0003718
0.0003701
0.0003685
0.0303663
0.0003627
0.0003506
O.C0035**
0.0003503
0.0003*62
0.0003*20
0.0003379
0.0003338
O.OC03297
0.0003E55
0.000321*
.. '.. 0.0003173
0.0003131
0.0003C90
0.00030*9
0.0003008
0.0302925
0.00028*2
0.0002760
0.0002677
0.0002595
.--.-.••; 0.0002512
'"••..:. 0.0002*30
'-.•: ;" 0.00023*7
0.0004*02
.; : 0.000*367
0.000*332
U. 000*293
0.000*263
0.000*229
0.000*195
0.000*161
0.000*127
0.000*093
0.000*009
0.0003926
0.00038**
0.0003762
~ •''.- • • . 0.0003682
.. ": ; 0.0003602
0.0003522
0.0003***
. 0.0003366
' - ••-. '-•-:- . 0. 0003290
...•'.• •• • ':'.' :".''•'•.•*. ''.: 0.000321*
. . -' \ : • < :':-; 0.0003139
0.000306*
0.0002991
0.0002918
..••-•-..••' '., •; »-,X...y :• : 0.00028*6
.•',.'.".'•;''•. - ' -'.'•• / •*••'-•>:. 0.0002705
':' : J : ' -.'-.•-?'•!>." 0.0002567
0.0002*32
0.0002300
0.0002172
, .... .:-..• . • ..:••••. . o.ooo<;o'.7
. :. , . ..:: '•. ! i ;> •• 0.0001926
•••• -' - ' .- :;', '-..". :; 0.0001808
                                                      KEAN DeVIATION  *    O.OC01712   ROOT  MEAN SQUARE DEVIATION
                                        [MODEL A]      RESIDUAL SUM OF SQUARES - O.IC021E-05"
                                                   .  KEAN PERCENT DEVIATION =  36.78317Z6
                     0.0001892
                                                      MEAN DEVIATION  -   O.OC01Z45    ROOT  KEAM SQUARE DEVIATION
                                       IKODEL B]       RESIDUAL SUM  OF SQUARES « 0.59380E-06
                                                      MEAN PERCENT  DEVIATION =  Z5.8966827
                     0.0001456
                                                      MEAN DEVIATION  »    0.0001238   ROOT  MEAN SQUAKE DEVIATION
                                       [MODEL C]       RESIDUAL SUM OF SQUARES = 0.5C217E-06
                                                      MEAN PERCENT DEVIATION =  27.5743^61
                     0.0001339

-------
           B'-~ TOHSHI "  152-G
                                     5 !'•> 71
                                                         [MODEL A]
                                             [MODEL B]
XCI1.GHS H2S04/GH C    RATEt CHS H2S04/GM C-NIN  CALCULATED RATE, CMS  H2S04/G1 C-MIN  CALCULATED RATE,  GKS HZS04/G* C-MIN
             [MODEL C]

CALCULATED RATE,  CMS HZS04/5H
O.OO165
O.C0331
O.C0496
O.CC661
0.00327
0.00992
0.01157
0.01323
0.01*38
0.01653
O.C2066
C. 02*80
0.02693
0.03306
0.03720
0.0*133
0.0*5*6
0.04960
O.C5373
0.05784
0.04199
0.06613
0.07026
0.07*39
O.C7853
O.C8266
O.OV093
0.09919
0.10746
0.11572
0.12399
0.13226
0.0007334
O.OC06086
0.0005618
0.0005072
0.000*760
0.000*526
0.000*292
0.000*962 .V-,. .... ' . . :..
0.000*018
0.0003902
0.0003667
0.0003*72
0.0303277
0.0003121
O.OC0300*
0.0002SB7
0.0002731
0.0002614
0.0002536
• • 0.0002*57
0.0002380
0.0002302
0.0002224
0.00021B5
0.0002107
0.0002028
0.0001951
0.0001872 , ,
0.0001795
0.0001717
0.0001599
0.0001522 .
O. 0002654
. 0.0002643 '., .::: . . rv>;: • '
0.0002631 ' , ' ' . ...
0.0002619
0.000260.8
0.0002596
0.0002585
-.„••••. 0.0002573: .- „•;.*..;;.'•:• • • <.. ,.:.:-
'"••• 0.0002561 '••',;.••>'"'! '" T-V-.-'.V. .-:
0.0002550 '•';: :.::.. i ''.'. . ' " ::
0.0002521
0.0002*92
0.0002*63
0.0002434
0.0002*05
0.0002376
0.00023*7
0.0002318
O.C002289
0.0002260 .:.,:• ' -., • -,.•:.. •••,.-.•. ,
0.0002231 ..:,'4'»' ."ii-.V " : '*' • l
0.0002202 -..-/' ; '; ' •'': •
0.0002173
O.C002144
0.0002115
0.0002086
0.0002028
0.0001970
0.0001912
0.0001854
0.0001796
: ;••: ;6. 0001738 : ..•:';*' .. ',;.;.' . . .-. "
0.0002987
0.000297* : ' '
O.OOOE9frl
0.0002 9', 8
0.0002935
0.0002921
0.0002908 , .'.
0.0002B95 : . • . -••;-•
O.C0028d2 ••-•'."
0.0002069
0.0002637
0. 000280*
0.0002771
0.0002739 - . • ' .:... : .
0.0002706 ' •'•' '•:.' ':*: •"•. '•''.' :.'-:•
0.000267* 	 -..'.
0.00026*1
0.0002608
0.0002576
0.0002543 •
O.C002510
0.0002473 ' - ,
0.00024*5
0.0002*12
0.0002380
0.0002347 , -.- ,. •, - •' •'•••. .. >v
0.0302282 ' : -,'' ,. ... • '.
'. 0.0002217 - ;'-. ;" ..:, '. •"••'
0.0002151
0.00020S6
O.OC02021
O.OB01956 • :
0.0003158
0.0003331
0.0003304
O.OUOJ251
0.0003225
0.000319B
0.0003172
O.OOD3146
0.0003055
0.0002991
0.0002Q28
0.0002365
0.0002S01
n.nOP?741
O.OU02681
0.0002620
0.0002561
0.0002501
0.00024*3
0.0002365
0.0002328
O.COC2272
0.0002216
0.0002160
'.*':• 0.0002052
.V'"i- 0.00019*6 -" 	
0.00018*2
0.00017*1
0.00016*3
0.0001547
                                 [MODEL A]
MEAN DEVIATION -   0.0000539    ROOT MEAN SQUARE  DEVIATION
RESIDUAL  SUM OF SQUARES =  0.17109E-06 .
MEAN PERCENT DEVIATION =   15.9290390
                                                                                                                0.0000811
                                              MEAN DEVIATION «   0.0000475    ROOT MEAN SQUARE  DEVIATION
                                 [MODELS]      RESIDUAL  SUM OF SQUARES =  0.11412E-06
                                              MEAN PERCENT DEVIATION "   16.0720062
                                                                 0.0000663
                                              MEAN  DEVIATION =   0.0000292   ROOT MEAN  SQUARE DEVIATION
                                 [MODEL C]      RESIDUAL  SUM OF SQUARES  =  0.67109t-07
                                              MEAN  PERCENT DEVIATION  =   8.2095785
                                                                                                                0.0000508

-------
       swi SUMBEH - 153-0
5 18 Tl
    (                                                       [MODEfTA]

XtU.GXS  H2SO*/G« C    RATE. GHS H2SO*/GH C-HIN   CALCULATED RATE. GWS H25oi/GN C-HIN
                                                             [MODEL B]
                                                                                      CALCULATED RATE, CHS H2SO4/KH C-MIN
[MODEL C ]
                                                                                                                             CALCULATED RATi, CMS H2SM/&N C-MN
O.OC61Z
0.00735
O.OCS57
C'. 00960
C. 01102
C. 01225
0.01531
t. oie37
0.02143
0.02450
C. 02756
0.03062
0.03363
0.0367*
0.03T91
0.04297
0.04593
C. 04699
C. 05205
C. 05512
C. 05818
0.0612*
C. 06734
C. 07349
0. 07961
0.0857*
C. 09166
C. 09798
0.10411
0.11023
C. 11636
0.12248
O.H47J
C'. 14698
0.15922
0.1714T
0.18372
0.19597
0.20E22
t. 22046
C. 23271
C. 24496
0.25721
0.26.946
0.23170
0.29395
0.30620
0.31845
0.33070
0.3429*
0.0178058
0.0159658
0.0141259
0.012523*
0.0109602
O.OU'96151
O.OU6 7C6B
0.0041921
0.0034123
0.0027599
0.01)24572
0.0022514
O.OC20&54
O.CC2D120
0. 01-19646
O.OOH230
0.001884*
O.OOU516
O.OOIB191
0. (,01702*
0.0017628
0.001~390
0.0316975
0.0016559
0.0016144
0.0015728
0.001525*
0. 0011838
0.0014363
O.C013S29
O.CC13355
0.0012379
0.0011S11
0.0010302
0.0009734
0.0008665
0.0007538
0.0006410
0.0005401
0.000*570
0.0003799
0. (,00326*
O.OOU2849
0.0002493
O.COD2255
0.0002077
0.0001899
0.0001662
O.OC.01543
0.0001*2*
0.001919*
0.0019131 ,
; 0.0019069
0.0019006
0.0018943
0.0018080
0.0018723
0.0018566 ' ... - " ; '
0.0018*03 '-..•.'; .-. . . . .
0.0018251 ' - .' •'.'
0.001809*
0.0017937
0.0017780
0.0017622 .;' ;
0.0017*65 .'• ... ,:. --.•:"
•0.0017308 ' • ' ".'
0.0017151
0.001699*
0.0016836
•• -..-• •-. . 0.0016679 ' ' .
.-•''• 0.0016522 •"*."..: ' ".' f .,:•"•'•";.
"'• ••'• • 0.0016365 :• •"'•..•-,'•"• , ! .,.' -
0.0016050
0.0015736
0.0015*22
. .'., i •.».;,•-;,-::. 0.0015107 ..-••••• .,.:•
.••••'.••'••"•. :..i .-:'•:• 0.001*793 • :- :/.". ''.,';•;.
0.001**78 >
0.001416*
0.0013850
0.0013535
.."<•, -.... „:....,: . ., 0.0013221 . •:•,;•.••,...:.,:..
•"- '.••-,- - 0.0012592 ' :i'-.*-" ; •-'.;••. A"
"... '.;,;; ..'r.^ 0.0011963 •".'."; -, > ;.;..
0.001133*
0.0010706
0.0010077
0.0009*48 , • , . , . :-,
. - - ' - 0.0008819 -•:*"-j:'-'.,; «".:" .."•'
o.ooo8i90 •'.'.-••'•' ;:•/.,..'.
0.0007562
0.0006933
0.000630*
.. . ,. .:..:. 0.0005675 .; , ::,:,u. ,'• . -
.' ' ...,.:• '• 0.0005046 -.••...'.- ',-.
0.0004418 ^ ' ^Lii; ' '
0.0003789
0.0003160
0.0002531
. ..'.-. • 0.0001902 .••..."•;. •'•.• ••'". ..•',
                                                                                                _0.0021755
                                                                                                  0.002168*
                                                                                                  0.0021613
                                                                                                  0.00215*1
                                                                                                  0.0021*70
                                                                                                  0.0021399
                                                                                                  0.0021221
                                                                                                  O.U021043
                                                                                                  O.OU2U864
                                                                                                _0.0020686
                                                                                                ~0.0020508"
                                                                                                  0.0020330
                                                                                                _0.0020152
                                                                                                  0.001997* "
                                                                                                  0.0019795
                                                                                                  O.C019617
                                                                                                ~O.OOD<.39~
                                                                                                  0.0019261
                                                                                                  0.0019083
                                                                                                  0.0018905
                                                                                                  0.0018726
                                                                                                  0.00185*8
                                                                                                  0.0018192 "
                                                                                                  0.0017B35
                                                                                                  O.OC17479
                                                                                                "0.0017123"
                                                                                                  O.OC16766
                                                                                                  O.OC16410
                                                                                                ' O.OC1605* '
                                                                                                  0.0015697
                                                                                                  0.0015341
                                                                                                ' 0.001*955
                                                                                                  0.0014272
                                                                                                _0.0013559
                                                                                                  0.0012847
                                                                                                  0.001213*
                                                                                                  0.0011*21
                                                                                                 "0.0010709
                                                                                                  0.0007996
                                                                                                _O.OC09283
                                                                                                  0.0008570
                                                                                                  O.C007653
                                                                                                  0.0007145
                                                                                                " 0.0006432 "
                                                                                                  0.0005720
                                                                                                  0.0005007
                                                                                                  0.000*29*
                                                                                                  0.0003582
                                                                                                  O.OOG2869
                                                                                                 ~0.0002156
                                                                                                  _0.002T5IT
                                                                                                   0.0027352
                                                                                                   O.OU271B9
                                                                                                 _ 0.002702*
                                                                                                   O.0026861
                                                                                                   0.0026698
                                                                                                   O.0026293
                                                                                                 "0.0025B90
                                                                                                   0.0025490
                                                                                                 _ 0.0025093
                                                                                                   0.0024699
                                                                                                   0.002*308
                                                                                                   0.0023919
                                                                                                   0.002353*
                                                                                                   0.0023151
                                                                                                   0.0022771
                                                                                                   0.0022394
                                                                                                   0.0022020
                                                                                                   0.00216*9
                                                                                                   0.0021280
                                                                                                   0.0020915
                                                                                                   0.0020552
                                                                                                 " O.OOH835
                                                                                                   0.0019130
                                                                                                   0.0018436
                                                                                                   0.001775*
                                                                                                   0.00170S*
                                                                                                   0.0016425
                                                                                                   0.0015778
                                                                                                   0.00151*3
                                                                                                   0.001*520
                                                                                                   0.0013909 '
                                                                                                   0.0012722
                                                                                                   0.001158*
                                                                                                   0.0010*94
                                                                                                   0.0009*53
                                                                                                   0.000t<.62
                                                                                                  ' 0.0007521
                                                                                                   O.OC06630
                                                                                                   0.0005791
                                                                                                   0.0005003 '
                                                                                                   OtO00*268
                                                                                                   0.0003587
                                                                                                   0.0002959
                                                                                                   0.0002387
                                                                                                   0.0001371
                                                                                                   0.0001413 "
                                                                                                   o.odoioi*
                                                                                                  _0.0000675
                                                                                                   0.0000*00"
                                [MODEL A]
       MEAN DEVIATION =    0.0007W1    ROOT  MEAN  SCUARF. DEVIATION
       RESIDUAL SUM OF  SQUARES *  O..17760t-03
       MEAN PERCENT DEVIATION =   39.2*94659
                                                                                                                       0.0019649
                                             MEAN  DEVIATION  =    0.0007402    ROOT MEAN SQUARE DEVIATION
                                [MODELS]     RESIDUAL  SUM  OF SQUARES  = o.i65i5E-03
                                             MEAN  PERCENT  DEVIATION »  47.5648651
                                                                                                                       0.0018948
                                             MEAN  DEVIATION  =    0.0006324    100T  MEAN SQUARE DEVIATION
                                             RESIDUAL  SUM OF SQUARES  = '0. 13940fc-03
                                             MEAN  PERCCMT DEVIATION «   22.1421509
                                                                                                                       0.0017408

-------
           Httt SUMEES » 157-0
                                        5 31 71
                                                             [MODEL..A]
[MODEL  B]
                                      [MODEL C]
XII),CMS H2S04/OM C    RATE,  CMS H2S04/GM C-MIN   CALCULATED RATF, GHS K2SO*/6M C~«I(t  CALCULATED RATE, GHS H2S04/GM C-HIN     CALCULATED RATE, GHS HJS04/SM C-MN
O.OC272
0.00407
O.OC543
O.OC679
O.OCSIS
O.CC951
0.01037
0.01222
0.01358
0.01693
0.02037
0.02377
0.02716
0.03056
0.03395
•. 	 _ 0.03735
O.OA075
0.04414
0.04754
0.0509J
'•':.• 0.05433
0.05772
0.06112
0.06451
0.06791
•;. -v . 0.07*70
: .' l ' 0.08149
», ' - O.OC828
O.C9507
0.10186
0.10866
; 0.11545
".-'- ' 0.17224
. 0.12903
0.15582
0.14940
0.16298
~ 0.17657
0. 19015
0.20373
0.21731
0.0042234
0.0039256
0.0025306
0.0014275
0.0012912
0.0012328
0.0011939
0.0011615
0.0011420
O.GU11096
O.OCH0.31
0. 0010966
0.00109C1
0.0010771
-- 0.0010706
0.0010576
O.CCIC447
0.0010382
0.0010517
. .' . 0.0.010107
•": : , 0.0010122
' 0.0009992
0.0009363
0.0009798
0.0009668
. 0.0009408
" '. . O.OCC9149
0.003SSS9
0.0008630
0.0003371
0.0008110
:. ' f. . .... 0.0007eSl - '
' . ••.' 0.0007592
0.0007397
0.0007203
0.0006673
0.00004B9-
! 0.00060J4 "
O. 0005516
0.0004996
0.0004477
0.0012000
•;.••• v. 0.0011956
. '.r^v 0.0011913
-•• ' 0.001187O
0.0011827
0.0011784
0.0011740
0.0011697 - *
0.0011654
0.0011546
0.0011438
0.0011330
•0.0011222
; . ... :'.,".-; O.OOU114
• v " "' '•'.'.:.• *"\" 0.0011006
s ..' ,.,.,: 	 0.0010898
0.0010790
0.0010682
O.C010574
' . ", ' 0.0010466
•* • 0.0010358
0.0010250
0.0010142
0.0010034
0.0009926
~\ 0.0009710 •"•' '! "' "
0.0009494 >
0.0009278
0.0009062
0.0008846
0.0006630
0.0008414
0.0008198
- > > , 0.0007982
0.0007766
0.0007334
0.0006902
1 . :"T?""r^TT!~~o. 0006470 ~" -—.— - —
•"•••• '•'••'. '':•.'': '..• 0.0006038 ' , •:
O.O005606
0.0005174
 0.
"o.
 0.
 p
 6.
 o.
_o
 0.
 0.
 0.
"o.
 0
_0
 0.
 0.
 0
 0.
 0.
 o.
"o.
 p.
 6.

 0.
 0.
"o
 0.
 0.
"o.
 0.
 0.
"o
 0
 0.
" 0
 0
 0
"o
 0
 0
""o
                                                                                                    OOU534_
                                                                                                    0013485
                                                                                                    001J436
                                                                                                    0013388
                                                                                                    001333?"
                                                                                                    0013290
                                                                                                    0013241
                                                                                                    0013193
                                                                                                    0013144
                                                                                                    0013022
                                                                                                    O012900"
                                                                                                    0012779
                                                                                                    0012657
                                                                                                    0012535""
                                                                                                    0012413
                                                                                                    0012291
                                                                                                    0012170 '
                                                                                                    0012048
                                                                                                    0011926
                                                                                                    0011804"
                                                                                                    0011682
                                                                                                    0011561
                                                                                                    0011439 "
                                                                                                    0011317
                                                                                                    0011195
                                                                                                    0010952"
                                                                                                    OC10708
                                                                                                    0010464
                                                                                                    0010221 "
                                                                                                    0009977
                                                                                                    0009734
                                                                                                    0009490"
                                                                                                    0009246
                                                                                                    0009003
                                                                                                    0008759"
                                                                                                    0008272
                                                                                                    0007735
                                                                                                    0007297"
                                                                                                    COO6810
                                                                                                    000632 3_
                                                                                                    0005836
                                      0.0016400
                                      0.0016292
                                      O.OC16184
                                      0.0016077
                                     '0.0015970
                                      O.UOl58t4
                                      0.0015757
                                     " 0.0015651 "
                                      O.OC15546
                                      0.0015283
                                      0.0015023
                                      0.0014764
                                      0.0014508
                                     "0.0014253
                                      0.0014001
                                      0.0013750
                                      0.0013502
                                      0.0013256
                                      0.0013011
                                      0.0012769
                                      0.0012529
                                      0.0012291
                                      0.0012055
                                      0.0011821
                                      0.0011590
                                      0.-0011132
                                      0.0010683
                                      O.OOI024J
                                      0.0009811
                                      0.0009.187
                                      0.0008972
                                     .0.0008565
                                      O.OOC8167
                                      0.0007778
                                     ' 0.0007397
                                      0.0006661
                                      0.0005961
                                     " 0.0005296
                                      0.0004667
                                      0.0004074
                                     ' 0.0003518
                                                 MEAN DEVIATION  =    0.0000383    ROOT  MEAN SQUARF DEVIATION
                                    [MODEL A]     RESIDUAL  SUM OF  SQUARES  = 0.5T829E-07
                                                 MEAN PERCENT DEVIATION »   4.8161469
                      0.0000406
                                                  MEAN DEVIATION  =   0.0001583    ROUT  MEAN  SQUARE DEVIATION
                                    [MODEL B]      RESIDUAL  SUM OF SQUARES = 0.88629E-06
                                                  MEAN PERCENT DEVIATION  »  18.1086273
                       0.0001591
                                                  MEAN  DEVIATION »   0.0002095   ROOT MEAN  SQUARE  DEVIATION
                                    [MODEL C]      RESIDUAL SUM  OF SQUAKE5 =  0.21175E-05
                                                  MLAN  PERCLNF  UtVIAUUN =   2
                       0.0002460

-------
                  BUS NUMBER - 158-G
6  1 71
                                                                [MCDEt-A]
                                                      [MODEL Bj
[MODEL Cj
         XIIItGNS H2SCH/GM C    RATE, CHS H2504/GM C-KIN  CALCULATED RATE, CMS" H2SOWGM C-HJN  CALCULATED RATEt  CMS H2S04/GH C-HIM  CALCULATE!) RATE, CMS H2S04/3K C-HH
CTl
0.00155
0.00310
O.OC466
e.or62i
0.0077&
C.CC931
0.01087
0.0 '-2*2
0.01397
0.01552
0.019*0
O.C?329
0.02717
0.03105
0.03493
0. 03681
0.0*269
0.0*657
O.OSO*5
•••.• 0.05433
0.05821
0.06210
0.06598
0.05986
0.0~'37*
0. 0^762
0.03538
; . . - 0.0931* ;
0.10091
0.1086?
0.11643
0.12*19
0. 13195
0.13972
0.1*7*8
0.0005393
0.000*289
0.0003675
O.OC'339*
0.0003180
0.0002995
0.00028*0
0.0002700 -•„:,..,:..
0.0002591
0.0002*63 • .
0.0002233
O.CCC2048
O.CC01S93
-C.CC.31775
-O.C0016A* -- •--
0.0001563 ••'..'.','
0.0001<.66
0.0001*13
O.OC013**
0.000129* '••'• -;• .-? • •. .
0.00012*3 ' "<:,'" V:< •:,'•'• . ..
0.0001198 . .' •.••;".''•.' ••;-
O. 0001161
0.0001124
O.OCOIOC7
0.0001050
0.0000991 ", „
0.000092*
0.0000872
0.0000821
0.0000769
0.0000725 .'•••.••• ••„..••
O.OD036S1 '* ' :"
0.0000636 ••-. '
0.0000591
0.0001TU
0.000170*
0.0001697
0.0001690
0.0001683
0.0001676
0.0001669
0.0001662
0.0001655
0.00016*8
0.0001630
0.0001613
0.0001595
0.0001577
0.0001560
0.00015*2
0.0001525
0.0001507
0.0001*90
, ... 0.0001*72 : :: -.'•: •• '- :.t : ,-' , . .
.h 0.0001*55 r ',:• • "'.•",' . •<:•'•.•:•* •-
:'• •" 0.0001*37 . .•>.•• . •'-- ••• ' ;;:.--%••..
0.0001*20
0.0001*02
0.00013B*
. O.OC01367
' 0.0001332
0.0001297
0.0001262
0.0001227
0.0001192
: 0.0001156 ,. ••.". V.: •. ; :.-,•:•; : :
O.OOOU21 " ' . -' , 05
                                                                           0.0000988
                                                       MEAN DEVIATION -    0.0000627   ROOT  MEAN SQUARE DEVIATION
                                         [MODEL B]      RESIDUAL SUM OF SQUARES = 0.28891E-06
                                                       KEAN PERCENT DEVIATION «  19.354'»617
                                                                                                                        0.0000998
                                                       MEAN DEVIATION =    O.C000497   ROOT
                                         [MODEL C]      RESIDUAL SUM OF SQUARES = 0.26197t-06
                                                       MEAN PERCENT DEVIATION =   5.0350761
                                                                                                  SOUARE DEVIATION
                                                                                                                        0.0000950

-------
         EOT BUH3ER - l60-C
6  9 71
                                                        [MODEL A]
                                                      [MODEL B]
[MODEL C]
XU),GMS H2S04/GM C    RATE,  GHS H2S04/GM C-H1N   CALCULATED RATE, CMS H2S04/GH C-H1N  CALCULATED RATE, GHS H2S04/GH C-H1N  CALCULATES f»»TE, 6-.' ;
' '• "••' 0.0005326 ... ?'".•--
: .. 0.0005305 . ' '. . . :".
0.0005282
0.0005259
0.0005236
. .•• :•.•"•:':••• ;•--• 0.0005213 : •. . . . - '
.---. -.-, - i': '••:.'. ' *.'"-. 0.0005190 ' ..V,.':*"' "c
. . •'•:. 0.0005133 :
0.0005076
0.0005018
.0.0004961
0.0004904
0.0004846
0.0004789
O.OOC4732
0.0004674
0.0004617
: :;;-,:',..- 0.0004560 . , :.'
:. :•.•';••::•/:..'•'•••'!•'>••. 0.0004502 .: : • -.,
-'•<-> •:., -•:,'• .:• 0. 0004445 s 'V. . / : '' '
0.0004388 	
0.0004330
0.0004273
< • 0.0004158 .; .' . .'
0.0004043 •>'•;!.•, . •
0.0003929 ",:'-'< :;
0.0003814
0.0003699
0.0003585
0.0006061
0.0006035
0.0006009
0.00059BJ
0.0005957
0.0005932
0.0005906
0.0005880
0.0005S54
O.OOC5799
0.0005725
0.0005660
0.0005595
0.0005531
0.0005466
0.0005401
O.O005337
0.0005272
0.00052O7
0.0005142 .
', Oi000507E
0.0005013
0.0004948
0.0004884
0.0004819
O.OO04690
O.C004560
0.0004431
0.0004302
0.0004172
0.0004043
0.000733!>
0.0007279
O.CCC7J2Z
0.0007165
0.000710J
.. ' 0.0007052
O.OD06943
0. 0006664
0.0006S09
0.0006473
0.000633S
• O.OOC62C4
O.C006072
0.0005941
0.0005812
0.0005684
0.0005557
' O.C005431
"' -. 0.0005307
'- 0.0005184
0.0005062
0.0004941
0.0004822
. y ..-.,<;. . s 0.00045S8
• .-'. •••" 0.0004359
;.:' . • • 0.0004135
o. 000391 r
0.0003704
0.0003497
                                              MEAN DEVIATION =   0.0000670   ROOT MEAN  SQUARE DEVIATION
                                   [MODEL A]    RESIDUAL  SUM OF SQUARES  «  0.21707E-06
                                              MEAN PERCENT DEVIATION =   13.8535995
                                                                            0.0000914
                                              MEAN DEVIATION »   0.0001035   ROOT MEAN  SQUARE DEVIATION
                                   [MODEL B]    RESIDUAL  SUM OF SQUARES  =  0.311-J26-06
                                              MEAN PERCENT DEVIATION =   24.1104126
                                                                           .0.0001095
                                              MEAN DEVIATION »   0.0001149    ROOT MRAN SQUARE  DEVIATION
                                   [MODEL C]    RESIDUAL  SUM OF SOUARSS =  0.39982t-06
                                              MEAN PERCENT DEVIATION =   26.84Hb60
                                                                            0.0001240

-------
                    FU3 :fUM2ES - 161-C
   6  10 71
                                                                  [MODEL A]
                                                        [.MODEL 3]
[MODEL C ]
           Xm.GMS H2S04/GM C    RATE,  CMS H2S04/GM C-MIN  CALCULATED RATE, CMS H2S04/GM C-HIN   CALCULATED RATE. GMS.H2S04/GH C-KIN  CALCULATED RATE, CMS H2S04/GH C-H1N
CD
0.00292
0.00438
O.OC584
0.00730
O.GC376
O.C1022
0.01168
0.01315
0.01461
0.01626
0.02191
O.C2556
0.02921
- - O.OJ286
0.03651
0.04017
0.04332
0.04747
0.05H2
"•';" 0.05477 ' ' .
0.0584E
0.0420B
0.06573
0.06938
0.07303
0.08033
: 0.08764
0.09494
0.10224
0.10954
0.11485
• . ' • 0.12415
; 0.13145
0.13876
0.14606
0.16367
0.17527
0.18988
0.0059734
O.OC42377
0.0030784
0.0019790
O.OC12460
0.0010481
0.0009455
0.0008722
O.OOOC429
O.OC080A3
0-QC07B43
0.0037623
O.OC075_•
0.0008051 : .>.. :..'•"•/ -. ':• '•'"•
0.0008817 •'•• ',-'•• '"-:•-'': :'.
0.0008782
0.0008748
0.0008713
..- -.,.. ...<..-; • 0.0008679 - -"C ,. »-
0.0008644
0.0008558 ' * :
0.0008471
0.0008385
.0.0008299
.-.' >.:.- :.- - • ••,:" O.oooa'212
; ' ':' • : 0-0008126
: . ,....:;' . • : 0.0008039
0.000/953 "' '
0.0007867
0.0007780
•-,-•/ ,;-?V;v •-, - -0.0007694 •:'•••'• (-»' •-..-' - ^•l"1.^
*>.-. ':,,•'•"• ' 0.0007607 "-' ..';'.•'. - .:••'•••'*:••
.'•''., • - . 0.0007521 -"•• : .: • ''it.'- "•*.
0.0007435
0.0007348
0.0007262
- =. •. - , ' -:i '•: ... :,- 0.0007089 , ' " " ""' 	
•:-;.'' ;'v,':':fV::-Kv'* 0.0006916
•• ••'?•••<• •"•'•-• '-•:-"•:- 0.0006744
0.0006571 	
O.OC06398
0.0006225
T: ';:-.;::::;.;.;;...;... 0.0006053 - 	 - —
•;'.'.- ':••; - 0.0005880
•: • .i . r •.-.•'••-.-• *••- '•-:- 0.0005707
0.0005534
0.0005189
0.0004843
•' . '-.»•* 0.0004498 .-' .• ..-,.•
0.0010061
0.0010022
:•': ,. 0.0009983
0.0009944
0.00099C5.
0.0009866
0.0009827
0.0009783
0.0009749
0.0009652
0.0009554
0.0009457
0.0009359
0.0009262
0.0009165
0.0009067
0.0008970
0.0008872
0.0008775
0.0008677 - •
-:/' o.oooasao
0.0008483
C.C008385
O.OC0828B
0.0008190 .
0.0007995 ." .- ': :
0.0007601 . ..;: -.
0.0007606
O.OOOT411
0.0007216
O.0007021
0.0006826 - >
0.0006631
0.0006437
0.0006242
a.0005852
0.0005462
:' 0.0005073
0.0012186
0.0012100
0.0012014
0.0011923
O.OOI1H43
0.0011757
O.OU11671
O.OOI15t8
0.001 1504
0.0011294
O.OOllOdf
o.ooioeei
0.0010676
0.0010474
0.0010273
'- - 0.0010074
0.0009877
0.0009681
0.0009488
; 0.0009296
0.0009106
O.OOOB917
O.OOOU731
O.OOOSS46
0.0008363
•;; , ••••• , , O.OOOBOOJ
.;., , • ' , ••:'-,' 0.0007649
0.0007)03
0.0006965
0.0006633
O.OOC6309
0.0005992
."•.'•'»: ... . 0.0005683
••• : 0.0005381
0.0005087
0.0004521
0.0003965
..•• 0.0003480
[MODEL A]
                                                        MEAN  DEVIATION =   0.0000561   ROOT MtAN  SQUARE DEVIATION
                                                        RESIDUAL  SUM OF SQUARES  = 0.13990E-06
                                                        KEAN  PERCENT DEVIATION =   8.0388994
                                                                                                                          0.0000651
                                            [MODEL B]
            MEAN DEVIATION *   0.0001371    ROOT MEAN  SQUARE DEVIATION
            RESIDUAL  SUM OF SQUARES -  0.67857E-06
            MEAN PERCENT DEVIATION =   20.5054016
                                                                                                                          0.0001434
                                            [MODEL C]
            MEAN DEVIATION =   0.0001771    ROOT KRAN  SQUARE DEVIATION
            RESIDUAL  SUM OF SQUARES  =  0.14490C-05
            MEAN PERCENT DEVIATION =  24.4635620
                                                                                                                          0.0002095

-------
         P,'JS 3UKBHR
                                    6 15 71
                                                        [MODEL A]
[MODEL B]
[MODEL C]
XII),GPS H2S04/G.1 C.   RATE,  GMS H2SC4/GM C-MIN   CALCULATED RATEt CHS HZS. '
0.08041 ; - ••:••
'•'•'', . 0.09772
0.05503
0.13234
0.10965
0.11696
i. 0.12427
. , _ 0.13158
0.13889
0.14620
0.16082
0.17544
0.0018122
0.0012529
0.0008129
0.0007085
0.0006570
0.0006190
0.0006041
0.00050^2
0.0005743
0^0005668
O.OOC5444
O.C005369
O.OC05220
0.0005146
0. 000*071
0.0005034
0.0005034
0.0004996
O.C004996
0.0004996
0.000499&
0.08C<-996
O.OU04996
0.0004996
0.0004996
0.0004996
O. 0004922
0.0004647
0.0004847
0.0004773
0.0004693
0.0004661
0.0004624
0.0004549
0.0004474
O.OC04325-
0.0004176
0.0003953
0.0006787
••-. ' ;.-•-•• 0.0006760
'--'•.,..,.'•-< v>v;:c. 0.0006734 '<•.".• :-~: ." " -
'• •'.'.' - 0.0006708 . : '. • ••'.'.•
0.0006682
0.0006656
C. 0006629
•• : ••• O.COC6603 ;..-.,.. a . ,
.-''.; :..'..V- ... 0.0006577 •:';.•..'."••"..",•.. .-
: • ''•'•' '"'•••: 0.0006551 '•-'" '•')' "
0.0006485
0.0006420
0.0006354
...::, ,\".. .„ 0.0006289
. ? ''. '-'• ,.'•!' ::':^;-r-- 0.0006223
• •.:'•, 'i:..'. '•' 0.0006158
0.0006092
0.0006026
0.0005961
O.OO05895 ' ' ' 	 "" '
0.0005830
0.0005764
0.0005699 	
0.0005633
0.0005568
0.0005502 	 Y 	
0.0005371 »
0.0005240 _j 	
0.0005109
0.0004978
0.0004847
0.0004716 • " ~, ,, '
0.0004585
0.0004454 ' :
0.0004323
0.0004192
0.0003930
... ,; .,:„, .-..,,.: ;.i.J, ,.,„,... .v, • 0.0003667 ,: • .-,,.,.. ..•:., .;••• jy-, ..-..•. . •
0.0007241
0.0007213
0.0007135
O.OC07157
0.0007129
0.0007101
0.0007074
0.0007046
O.OOC7018
0.0006990
O.COG6920
O.CC06S50
0.0006780
0.0006710
0.0006640
0.0006570
0.00065OO
0.0006430
0.0006360
O.OOC6290
0.0006220
0.0006151
0.0006081
0.0006011
0.0005941
0.0005871
0.0005731
0.0005591
0.0005451
0.0005312
0.0005172
0.0005032
0.0004892
0.0004752 :
0.0004612
0.0004473
0.0004193
": 0.0003913
0.0003499
0.0008419
: 0.0008380
0.0006120
O.OOUIJ2&1
O.ODOU701
O.OOCB142
0.0008CB4
0.00(Jh025
: . 0.000?V66
0.0007821
0.0007677
0.0007534
••'••• 0.000731J
.. ; . 0.000/252
0.0007113
0.0006975
0.0006839
0.0006703
0.0006569
. . ' j'.' . , 0.0006436
: 0.0006304
0.0006174
0.0006044
0.0005916
i . •-,-.'• * .'. ' .••-•• 0.0005790
: s - ' « -, 0.0001540
: •'•-.i.'-f'-:. - '• ' : " 0.0005295
O.OOO^i
0.00048^0
0.0004591
. ".-. ' ••--.-. ' • • 0.0004366
.,' •:>' '•:': • ; '• "" 0.0004147
• '-••-.• V?;'--: 0.0003932
0.0003723
0.0003519
0.0003127
• 0.0002756
                                              MEAN DEVIATION =   0.0000628    ROOT MEAN SQUARE  DEVIATION
                                 'MODEL A]      RESIDUAL SUM  OF SCUARES = 0.17069E-06
                                              MEAN PERCENT  DEVIATION =  12.2738953
                     0.0000730
                                              MEAN  DEVIATION -   0.00009*3   ROOT KEAN  SOUARE DEVIATION
                                 [MODEL B]      RESIDUAL SUM OF SCUAKHS  = 0.36657E-06
                                              MEAN  PERCENT DEVIATION =  18.3562317
                      0.0001070
                                              MEAN DEVIATION »   0.0001336   ROOT KEAN  SOUARE DEVIATION
                                 [MODEL C]      RESIDUAL  SUM OF SQUARES  =  0.75555E-06
                                              MEAN PERCENT DEVIATION =  26.1*30359
                      0.0001537

-------
                   APPENDIX A-8

        COMPARISON OF MULTIPLE REGRESSIONS
       TO 6 INCH DIAMETER FLUIDIZED BED RUNS
                                                    Page

Westvaco Model by Stepwise Regression Compared       121
  to Continuous S02 Sorber

Westvaco Model by Multiple Regression Compared       128
  to Continuous S02 Sorber

Westvaco Model by Multiple Regression (Loading       135
  Factor Order) Compared to Continuous S02
  Sorber
                        120

-------
             APPENDIX A-8-1

  WESTVACO MODEL BY STEPWISE REGRESSION
    COMPARED TO CONTINUOUS S02 SORBER
             Westvaco Model
dXv  _  ,  _-E/RT n    xv N Yn   Ym  Yp
 dt      K e      U " 0.38;  S02 Y02  H20
where  -E/RT = 5520°R

       n     =0.50

       m     = 0.63

       p     = 0.73

       k     = 1.59(10-4) gms. H2S04/gm. G-min.
                   121

-------
        S02 SDRBER  DESIGN

  RUN NUMBER      SA-21   DATE   6  7  71

 _Ji'LAk CAP(HiN_RATiE j=	?_*J!.1 J?_ .Mii/JJR,				

  HEIGHT OF CARBON/STAGE =    2.25 INCHCS ,-   '.:;;;;*;;.'..,.,;.».--,,..,„,,:,.,	-. ..,.-..-,.•,.>•»•..    ,.,.•   .......
  DIAMETER OF VESSEL =  6.0  INCHES       '   -  -  *  ' '•'•   •••••:•••-.••.-•>:<. •/*•>•' •:,..;.•. v. •.-.•./. «..*•. i.1^..-..   .....,.,••:.-,., s.
  CARbON USED =   96324.
  TOTAL  GAS I LOW  RATE =      1247.  SCFH
 _I_NLEJ_SO? Cf)NCFNTRAT_IpN_^__	20p_2i__PPM _
r INLET  NO c'OMCfcNTRATIO"N"=     " ISO.  PI'B
  IMLET  02 VOLUME FRACTION  =  0.0420
	INLr.LJI2tl_VpLf)ME_FRACJ | ON *  Q...13QO. :... .	
  UUTLET S02 CO'-JCENT RAf'l IJN  =       165. PI'H
^_T_EM PER AI U R. C
STAGE
r i
2
3
i 6
[ 7
8
9
	 0.22... .
= 200.0 DEC, . F
S02 CONCENTRATION
PPM
2009.
1799.
1574.
1357.
1093.
847-
. . 608. 	
3B6.
200.
165.0001

ACID LOADING
. LBS ACIU/1.0 CARBON
0.17BB
0. ll>42
0. 1279
0.1002
0.0715
0.0147
0.0
0.0
0.0
  TOTAL  CARBON  REQUIRED  =      20.75  I NOIL'S
  TOTAL  STAGES  REQUIRED  ASSUMING  2.25  INCHES  CARBON/STAGfc = 9.22
  SPACE  VELOCITY  =      3672. l/HR

 .PRESSURE DROP ACROSS  CARBON -	io.3i». JNCUC-S HZO
  PRESSURE DROP  ACROSS  PLATES =      5.19  INCHES M20
  TOTAL  PRESSURE  DROP ACROSS STAGES  '     15.56 INCHES  1120

  RATECI1 )=COEFF  * (1-X I 1 1/XS) **A  *  (YSCI2*«D)  * (Y02**C) *  (YH2C**D)
 	WHE.R-E_C.OtCF.5.K <• CXPJ-E/H*! I/ lTt/.601 I I	
           T«     200.         XS=     0.38       YS02=                 Y02=    0-OH2        YH2O    0-130
       _:;E/.R_i	5.5.aQ.		...A"	l_.(jQ.O	B=	0.400	    .C*	0.6.30.  '	0; 	0.73(L
           K«0.000159
                                                  122

-------
       S02  SORUER DESIGN

  RUN NUMBER     SA-22    DATE  6  15  71

  TOTAL CARBON RATE  =   3. 260_J.RS/HR
•OUTLET  CARBON LOADING »""o". 2 2V/9 "Vll'S" AC Fl)
;  HEI&IH  OF  CARHON/STAGE -   2.35  INCHES
;  0.1 AHE TEJ>;>* ^, f'^f.:*:+^& •"?;»•'-'' <:-.;>r''^
 I  PRESSURE.. DROP..ACRgSS_..CA^fiON....-/::::r::.t;lPy8.'J;:>;i-NCHES";)H2U .-^:if^^^!^£^afM^^l^-i::i^f:^P-'^<^^^
   PRESSURE OROP ACR~OS~S PLATtS =      5.**  INCHES H2U
   TOTAL  PRESSURE  DROP ACROSS STAGES  =     16.33  INCHES H20
 £—__„_,_		   ———
 !
 ^	RATE EXPRESSION  USED IN OESIGN CALCllLATIONS
   RATECU l^COEFF  *  ll-XI I )/XS)**A  * (YS02**D)  * (Y02**C1  *  (YH20**[)I
   -__BHERE. COE F F ' K  «  E X P I -f. /R * I 1/ I T * *60 II I	 „
           T'    200.         XS-     0.38   .    YS02«       .     ,   Y02=    0'0>42       YH20=    0-130
       _-E/R=	.ss?p,_	•;;.;,:.,...A».: „,..L-QOQ-'        •:»*•  : o.*oo	„	„_!>_	^*AQ	   _.^f....^_P±J3p
           K-o".obb"r59        ~                             -----                  	-.
                                                123

-------
       S02' SORBER DESIGN
  RUM  NUMBER
                 SA-23   DATE  6 16 71
  TOTAL CARBON RATE =  3.350 IBS/MR
OUTLET CAROUN LOADING = 0.16660 LUS AC I D/IB CARBON.,.,; :.;.,;;. ;:;j";^.<;::";;!:', :.;:.•: '-V ••: • >•.-; > T^;', -'-i '•V,:;:::>V'^::!-'\^::i:':J'--W:it;i:;'";
HEIGH1 Of- CARBON/STAGE = 2.40 INCHES.. :'^^V£'^^?'^ >:&&^:r":> .. W?; ^Zl^'^^ff'.'*- ,
: DIAMETER OF VESSEL * 6.0 NCHES .- /V-^:^S;^l::J^
CARBON USED = 96324.
TOTAL GAS FLOW RATE = 1106. SCFH
INLET SCI2 CONCENTRATION = 2009. PPM
INLET NO CONCENTRATION. = 150. PPK .
; INLET 02 VOLUME FRACTION = 0,0420
: INJJLT H?O voLyME FRACTION = 0.1400 :
OUTLET SU2 CONCt NTRAT I UN = 91. PPM
TEMPERATURE •= 200.0 DfC. F

••• :i::- ••' '*f':i'!>'*^''VV«* TOTAL CARBON REQUIRED » 20.36 INCHES * - 	 	 	 ' 	 ,.,..
  TOTAL STAGES RFUU1REO ASSUMING 2.40  INCHES  CARBON/STAGE = 8 ..48

        yti nr I ry g	3J10   I/HP.
^PRESSURE DROP ACROSS CAKBUN
j' PRESSURE OkOP ACRQSSIPLATEl
       10.ia  INCHES  HZO
  TOTAL PRESSURE DROP ACROSS STAGES  =
                                          15.27  INCHES H2G
     RATE EXPRESSION USED  IN DESIGN .CALCULATIONS
  RATECII)=COEFF * (1-X(I)/XS!*«A  *  (YSM?**G>  * (Y02**CI * (YH20**D)
     WHERE CUEFF = K * EXP(-E/R*I I/(T+460 I) I
          T-    200.
       -E/R*   5520.
      ...._	K°-Q...O.Q015
-------
      S02 SOKUER DESIGN
 RUM NUMHCR
                SA-24
                         DATE  6 16 71
 TOTAL CARBON RATE -   3.190 LBS/HR
 OUTLET CAKHUN LOADfNG"=="o".lHllJ'. LBS'
 HtlGHT OF CARBON/STAGE  =    2.45 INCHES ;
JMAHETCR OF VESSEL =	6.0 INCHES ,!<• y>;.,..
 CARBON' USED =  96324.
 TOTAL GAS FLOW RATE  =       965. SCFH
 INLET S02 CCNCr(ifRATION =	39B2. PPM
 OUTLET S02 CONCENTRA1 ION
                                 10?8. PPM
_Ii"EIM.iy?E_
     STAGE
               250.0  OEG.  F
            SO2 CONCENTRATION
                    PPM
                                     AC 1 0 LOADING
                                  LCS ACIO/LD CARBON
                                     .      O.IB83
2
3
5
. 6 '.-y:,--- '•
7 ."•;•••,:'.
8
9
1 1 ... --.,::,; •
\ '0.65 ' 'C:y-:;;
}762.
35?7.
3277.
3012.
-•>• 273-i.
2150.
1848.
1544.
•f*' •• 1254.. .:••;", ::.V/':i.,::vi,,-:. .-i.:
. 10 78. 0002 ]Ki;;X&&^
0. 1 701
0.1507
0. 1300
0.10H2 ;. . ...,<. :. ,-;.:,*VJ;..V, ;•.--.-- ..•..'• .:-:,...<. - .-:. .>.^; " .. ; -^ '•.:.. '
0 . 0853;. :;: :/:':-.;:.- ! ';. ^^•^^'•^•i .V '!"(• f'::^ ''.:• :''••••; V,! -:' '•, . ':<»™-:S.''::^>:' "-,':'. \ • .:•
0.0614 •::''i'-':r:S,'-:-I:-:-cif';:.i:i^':::.v :'-;:-iii^t.''J'.* '•'•''-.'' •^y:i--f:..::-l^}';! ,
0.0369
0.0119
0.0
;So;|g|||»
TOTAL CARBON REQUIRED
TOTAL STAGES REQUIRED
                              20.55  INCHES
                                             .-,CARBON/STAGE. af
 PRESSURE  DROP  ACROSS CARBOM
 -PREi5u&E__DBPJ:Lj'C!?.o.S S..,.PL A T e s_
                                  U.27 INCHES H20
                                   7 .It 1 NC H t SH2 0
 TOTAL PRESSURE  DROP, ACROSS STAGES
                                        21.*1 INCHES H20
    RATE  EXPRESSION USED IN DESIGN CALCULATIONS
 RATEC(M=COEFF,  *  1 1-X 1 I)/XS )**A *  (YS02**[()  *  (Y02**C) * (YH20**U)
    HHERE  CriEFF*.K  *  EXP (- C/R* ( U I T+460 ) ) ) :      '           :   -:
    T=    250.
 -E/R=   5520.
	^KFa..000159_
                            xs
                                   0.38
                                  I. 000
                                                    O.'.OO
                                                                 Y02 =
                                                                   C =
                                                                         0«0't6
                                                                         0.630
                                                                                     YH20 =
0.1 30
0.7JO
                                            125

-------
       S02 SORBtR DESIGN

  RUH NUMBER     SA-75   DATE   6  17  71
 _LP-IH       _.     __ -      .
  OUTLET CA"RbON~ I fMIMNG -  0 ."liJOl 7 "llilT AC I 0/LI.I CARBON
  HEIGHT OF CARrtON/SUGt =    2.35  I'MCHT-r
  DIAME.IEK QFJ/FSSEL - ___ 6.0 .INCHES ______ ................
  CAKUUN USED =963/4.
  TOTAL GAS FLOW RATH =      109'..  SCHI
  INLET S02 CONCF'-IIKATJUN  ;___  202b.  PPM
  INLET "NO "ctiWcrMTRAT ION ' '=     " 150 .
  INLET 0<> VOLUME FRACTION =   0.0410
|__INLfcT H_20_VOLLme (-RACT I ON_i._OjJ[JjOO
        " "             ""      "
                                        PPM
  TEMPLRATURH_=_250.0 PEG.  F-
r S
STAGE
I
2
3
r 	 ~r
? 7
8
9
10
0 . .5 7
02 CONCENTRATION
PPM
2020.
Ibii.
1679.
1^)00.
inn. '
960.
7U6.
619.
411.0000
ACID LOADING
LDS ACIIJ/LI) CARBON
. . 0 . 1 2 02 .••'
0. 1124
0.0962
0.079H
. •'.. '. . 0.0467
•'- "<*•• ••'=;'- '0.0304
0.0145
0.0
0.0
0.0.
  TOTAL CARBON REQUIRED  =      2A.36 INCHES
  TOTAL STAGES REQUIRED  ASSUMING 2.35 IMCHE5. CARBON/STACE =10.37
  SPACE VELOCITY  -
  PRESSURE UROP ACROSS  CARBON  =     12.IB INCHES H20
  PRESSURE DROP ACROSS  PLATES  *      6.09 INCHES H20
  TOTAL PRESSURE DROP ACROSS  STAGES =    IB.27 INCHES H20
     RATE EXPRESSION  USED  IN DESIGN CALCULATIONS

  RATECt I » = COEFF *  Il-Xt I )/XSI**A * (YS02**8) *  (Y02*<-C )*JYH20**0)
     WHtRE
* EXP(-t/R*( l/IT-1460) ) )

                0.38
       -E/R-
          K=0.000159
                                                      0.400
                                                                     c=
                                                                          b.630
                                                                                          =
                                                                          0.130
                                                                        " 07730 "
                                              126

-------
       S02  SORBER DESIGN

 RUN NUMOER     SA-26   DATE  6  18  71
TOTAL CARBON RATE = 3.400 LBS/HK
; OUTLET CARBtJN LOADING * 0
! HEIGHT OF CARIJON/STAGE =
: DIAMETER Uh VESSEL = 6.0
CARBON USED = 96324.
TOTAL GAS FLOW RATE «
INLET S02 CONCENTRATION =
1 INLET NO CONCENTRATION =
{. INLET 02 VOLUME FRACTION
|_ INLET H20 VOLUME FRACTION
OUTLET S02 CONCENTRATION
TEMPERATURE = 200.0 DEC.
| $02 CONCENTRAT
i STAGE PPM
I 	 1 2055.
2 lf>31.
3 1595.
4 1350.
f 5 1100.
| •*.; 6 ... 851.
i . :/ 7.1. 	 611.
8 390.
9 200.
10 60.
i 0.14 46.0000
i 	 •-'- 	 	 -- 	 •'
.IH'JZS LUS AC1U/LU .CARBON , :
2.30 INCHES
.INCHES - ....,'•
1186. SCFH
150. PPH ' •. :. •. .: .•••••: ..-..'.• ••"V:.:.:^-;: T" T.v:- •:.;-::":: ":.;"- "•: . -•-' ••""':-[1,..' -'•'••-. - •
= • 0.0430 .:'••••• -' ~^^Q^'\^'^^^^^?^^^^-^ -: :'&^^^.^:'. • •• .
- n Hftfi'-^'s- • -•-••^--.:*^^ •••V.-<.:v'-x^sr:.^;^^^;/:.v-.^i«*i: •:•:..• -«i'.-^.-:>- ^•.^••.-. ,., . .'
....... O.» IjUU. v>.:' ,<:.:.:••....,. ........ ; .^v^.. S: »^i-»' ;». .; ;: i '•:.^.v.;;. ..C^.T-'.;. -'..I •,. v'.t ,"•'. .V- .• .. .
= 46. PPM
F
ION -'.-. ,ACtO LOADING ; ,•:;
LBS ACID/LB CARDON :
'" . ... .. " • :•'.. .. 0.1853 . , •- ' -••;/•. -•••:•
0. 1639
0.1414
0.1180
: 0.0941 ' ' ' ...
: ,,, , 0.0704 •.>'."
. ' ,.,"". '. :.:';.-, ' 0.0475.
0.0264
0.0083
0.0
0.0
  TOTAL CARBON REQUIRED =      23.31  INCHES
  TOTAL STAGES REQUIRED ASSUMING  2.30  INCHES CARBON/STAGE =10.14
  SPACE VELOCITY =  -   3110.  l/HH
  PRESSURE DROP ACROSS CArtftON  =     U.66 INCHES H20
  PRESSURE DROP ACROSS PLATES  «      5.83 INCHES H20
  IP!AL_PRESSURE PROP ACROSS STAGES =   	17.48 INCHES H2p
r	  " ~™~	
     RATE EXPRESSION USEU  IN  DESIGN  CALCULATIONS

  RAJECiJ )=COEFF * J1-X(I >/XSI**A  «  (YS02**B1 » (Y02««C 1  *  (YH20«*D)  ________„„______	
r^"  HHtRE CtlEFF = K" *"CXP(-E/R*(l/(Ti460l H                            ~        "             "" :"   ..:

\  ' ':>,'••   T«	, 200. _  ....".'. :.XS«  	0.38 '     VSU2--	YQg" .... 0.0^.3 '	YH20=    0.1 3JL
  ~"    -E/R=   '55201""         A«~  1.000         B«  "0.400          "C=   0.630         D=  " 6~~."/30
          K=0.000159
                                            127

-------
             APPENDIX A-8-2



   WESTVACO MODEL BY MULTIPLE REGRESSION

     COMPARED TO CONTINUOUS S02 SORBER
              Westvaco Model
 dXy     ,   -T       Xy x  n    m
 __  =  k e
where -E/RT = 5416°R



      n     =0.48



      m     = 0.62



      p     = 0.73



      k     = 3.32(10-4) gms. H2S04/gm. C-min
                   128

-------
       S02  SORBER DESIGN

 RUN  NUMBER     SA-21   DATE  6   7  71

 TOTAL .CA.UJ}.OiLKAIE..«  2.910 LBS/HR	
 CUTLET  CARBON LOADING = 0.17885  LBS ACID/LB CARBON
 HEIGHT  OF CARBON/STAGE =   2.25  INCHES
_JCLl AM EIE R  0 F.._V E S S E L.. »_. 6. J). 1 .MCHtS	
 CARBON  USED =  96524.
 TOTAL GAS FLOW RATE =     1247.  SCFH
_l;JL£J..SUZ.-COJJCJ:.NIRA.IJJMi_ =	.2009, J>PJ1	
 INLET NO  CUMCENTRATION =       150.  PPM
 INLCI 02  VOLUME FRACTION »  0.0120
._I;
-------
      S02  SORBER DESIGN

 RUN NUMBER     SA-22   DATE  6 15 71

_TOTAL CARBON  RATE  =   3.260 LBS/HR
 CUTLET  CARBON LOADING = 0.22479 LBS ACID/LB  CARBON
 hCIGHT  OF  CARBON/STAGE =   2.35 INCHES
 L.IAKcTE*  OF VESSEL =.6.0 INCHES		
 CAKBCN  USED =  96324.
 TOTAL GAS  FLOW RATF  =     1141. SCFH
 INLFT SD?  CONCtNTKAT I UN « __   .3946. PPM	;	
 INLbT NO  CONCENTRATION *~	150. PPM
 INLET 02  VOLUKL" FRACTION *  0.0420
 INLFT M20  VOLUME FRACTION. = _0.1300	.	
"OUTLET  502 CONCENTRATION =     1151. PPM

 TEMPERATURE = 200.0  DEC. F __           	
            S02 CONCENTRATION        ACID LOADING
     STAGE          PPM            LBS AC10/LB  CARBON
	      1            3946,   _        	0.2248.   .
         2            3658.                  0.1972
         3       .     3333.                  0.1661
         4   __       2970.	    	0.1314	
         5            2574.                  0.0935
         6            2151.                .  0.0530
	7	17.14..	0.0_1.11
         8          *  1277.                  0.0
     0.31        1151.0005                  0.0
..TOTAL CAP.BON...REQU.IRED..=	_l.9_v53...!.NC.Ht.5	
 TUTAL STAGES REQUIRED ASSUMING 2.35 INCHES CARBON/STAGE = 8.31
. S P AC E. V E UiciT.V..=	3 5J_Q.  .
L/HfL.
 PRESSURE 0VROP  ACROSS  CARBON =     9.76  INCHES H20     .  ,
_PRESSURF,. DBOP. ACROSS  PLATES =  .   4.,8y..JNCHES H20    ..._,
 TOTAL PRESSURE  DROP ACROSS STAGES =     14.65  INCHES  H20
    KATE EXPRESSION  USED  IN DESIGN CALCULATIONS
 RATECII) = COEFF *  11-XI II/XS>**A * (YS02**B) *  (Y02**C)  * 
-------
      S02  SORBER DESIGN

 RUN NUKbER     SA-23   DATE  6  16  71

JOWL. CARBON P.AT.E =  .3.3SO LBS/HR  ______  _    ___
 UU11ET  CAKBOfl LOADING = 0.16660  LBS ACID/LB CARBON
 HEIGHT  l)f: CARBON/STAGE =   2.40  INCHES
_i,IAMET£K  OF. VESSEL .? ____ 6..Q_LiCU£5
 CARBON  UitO -  96324,,
 TOTAL  GAS FLOW RATE "     1106. .SCHH
 LNkEJL  $Q2._C_QNCE.NI.f.; .....
_. 0.0123 \
0.0 i • •
0.0
:-.:V:. ., :,:.•: : ..-.- '•'. ' '•:'•. , • ' • -. ' '
•••••"•• -'• ' ' '• • 	
  TOTAL  STAGES REQUIRED ASSUMING  2.40 INCHES CARBON/STAGE  =  8.25
V  PRESSURE  DROP ACROSS CARBON =      9.90 INCHES H20     -:.'•
LERESSURf .BRUP-.ACROSS.. PLAT£S._=	_..4_, 9i_JjNI.CHE5_H2.0	
  TOTAL  PRESSURE DROP ACROSS STAGES  =     14.85 INCHES H2U
     RATE  EXPRESSION USED IN DESIGN  CALCULATIONS
^ATECI I I=COEFF * ( l-X( I ) /XS 1 **A * (YS02**E» * (YOJ
WHERE COEFF = K * EXPI-E/R* ( I/ ( T*460 ) ) 1
T =
-E/R=
200.
5416.
XS =
A»
0.38
1.000
Y02*
B=
>**C) *
~oToT£
0.480
                                                              vH2**l
YH20=
   C«
                                                                        0.130
                                                                        0.620
                                                                                         0=    0.730
                                             131

-------
      S02 SORBER DESIGN
 RUN NUMBER
                SA-24   DATE  6  16  71
 TOTAL CARBON RATE =  3.190LBS/HR  ........ _ ..... _
 OUTLET CARBON LOADING - 0.1883'. LDS  ACIU/LB CARBON
 HEIGHT OF CARBtlN/STAGE
                            2.45  INCHES
_DJAK£ICft OF VESSEL -  6.0  INCHES
 CARBON USED =  96324.
 TOTAL GAS FLOW RATE --
_INLET SU? CONCENTRATION^
 "INLET NO CONCENTRATION «
 INLET 02 VOLUME FRACTION =
 INLET H2U VOLUME FRACTION
 OUTLET S02 CONCENTRATION -
                            965.  SCFH
                                3982. PPK
                                156..  PPM
                             0.0460
                              0.1300 __
                                 1078.  PPM
JLEMKERATURE
STAGE
	 .. 1 ...
2
3
4



5
6
7
8
9
10
0.32
= 350.0 DEC. F
S02 CONCLNTKA1 ION
PCM
5982,
3720.
3439.
3139.
2823.
2495.
2157.
1317.
1480.
1170.
1078.0002

ACID LOADING
LBS ACID/LB CARBON
0-1883 _^
0.1667
0.1434
0.11B6
0.0925
0.0654
0.0375 i
0.0093 /
0.0
0.0
0-0 ., „'.:•:„ • ... ,.',.. „ - ;
 TOTAL CAR60N REQUIRED =     25.28  INCHES
 TOTAL STAGES REQUIRED ASSUMING 2.45  INCHES CARBON/STAGE  =10.32
 SPACE VELOCITY =
                      2332. 1/HR
 PRESSURE DROP ACROSS CARBON =    12.64  INCHES H20
 PRESSURE DROP ACROSS PLATES =     6.32  INCHES H20
JTOTAL PRfcSS.URfc_ DROP. ACROSS .STAGES.. =	18.96  JNCHCS  H2CL	
    RATE EXPRESSION USED IN DESIGN CALCULATIONS

.RATECt I ) = COEFF * ( 1-X I I I / XS I »*A . * 1 YS02**6 ).. *_
    WHERE  COEFF=K * EXPI-E/R* ( I/ ( T+460 ) ) )
         T= __..250. ...... ______ XS* __  _0.3fi__     Y02=
      -E/R=   5416.         A=    1.000         B-
         K=0. 000332
                                                         *.IYH20**DI
                                                     0.0'(6   __
                                                     0.480
 =  ,0.130	  ..  				
C=   0.620         0=    6.730
                                           132

-------
       S02 SCIRBER DESIGN

 RUN NUMBER     SA-25    DATE  6 17 71

_JQTAL_CAR_BQN _RALE_f_-3.210_LBS/HR	.	
 OUTLET CARBON LOADING =  0.12817 LBS AC1D/LB  CARBON
; HEIGHT OF CARBON/STAGE  =   2.35 INCHES
_D.I A.METE.R .OF. .V£SSEL^=__6.,ja._JJi.Clt£S	
 CARBON USED -  9632'..
 TOTAL GAS FLOW RATE -      1094. SCFH
  INLET_SQ2 CONCENTRATION  -   _ 2028._ PPM_ __ _ _	
rINLET NO CONCENTRATION  =      150. PPM
  INLET 02 VOLUME FRACTION =  0.0410
_JNLF.T H.20 ..VOLUME. F.RAQJ.I.CN__=__0J.13.00			
 OUTLET S02 CONCENTRATION =      411. PPM

 TEMPERATURE = 250.0 DEG._F	
"            S02 CONCENTRATION        ACID LOADING
i     STAGE         PPH             LBS ACIU/LB CARBON
;	.1	2.Q28->	0.. 128^	
         2           1834.                 ' 0.1104
         3           1636.                   0.0923
,	4	.	14.37.;	.0,0741. _
                     1239.                   0.0559
                     1045.                   0.0382
                            	'  •-	  0.0210	
                      679.                   0.0047
                      515.                   0.0
                 _4 H..OOO-0 ,  ,   ,	0 ,J)	
  TOTAL CARBON RtQUlRfcD  =      22.80 INCHES
  TOTAL STAGES REQUIRED  ASSUMING 2.35 INCHES CARBON/STAGE = 9.70
  SPACE VELOCITY = ,     2934.  1/HR
                                      ^4.0_I NCME.S_H2Q	
  PRESSURE DROP ACROSS  PLATES =     5.70  INCHES  H20
  TOTAL PRESSURE DROP ACROSS STAGES =     17.10  INCHES H20
   .._RAT.£..£XP.R£5S1QN..1JSED_..IN^DES.LGN_£A.LCU1A_TJO_NS-
  RATEC(I) = COEFF *  (1-X(I I/XS)**A * (YS02*»BI  *  (Y02**CI * (YH20**D>
 ___ WHERE COEFJ:=K.*_..EXP.(-E/R*iayj.T.±4.60.JLU	-	—
          T=    250.         XS=    0.38        Y02=    0.041      YH20=    0.130
               5416^	^	A=	L..OaO-	BL-.	Q.4dO	£±	O..I.6.2P	..JJ? .-.0
          K=0.000332
                                              133

-------
       S02 SURBER DESIGN

  RUN NUMBER     SA-26   DATE   6  18  71

_JOTAL  CARBUU RATE =  3.400 LBS/Hft            _   ,. _		
  CUTLET CAkl'CN LUAU1NG = O.IB528  LBS ACID/LB CARBON
  HEIGHT cr LARHOM/STAGE -   2.30  INCHES
  C1AMETER Or VESSFL -_ 6.0  INCHES _			_.	
'CARBON USED -  9&324o
  TOTAL  GAS ROW RATE =      1106.  SCFH
  INLET  SC2 CONCENTRATION =     2055. PPM       	 _j	
  INLET  NC CONCEPT RAT'i ON =      150'.  PPM
  INLET  0? VOLUME FRACTION =   0.0430
  INLET  H20 VOLUME TRACTION  -   0.13_00	.	,	
  CUTLET SU2 CONCENTRATION -       46.  PPM

  TI-MPiRATURl  - 200.0 !)F&. f
             SU2 CONCENTRATION         ACID LOADING
      STAGE         PPM            LBS  ACIU/LB CARUON
         1           20^5.      		P.je>3	'.	
         2           1(306.                   0.1615
         3           l'.''.c>.                   0.1366
         4           12/7.                   0. 1111  _
         .5           1010.                   0.0856
         (S            75?.                   0.0609
         7	___51$.   _      ^	   	O.OJ82	
         8            308.                   0.0185
         9            H5.                   0.0030
      0.90_      ... .46.0000	Q.O				



  lofAL  CARBON REQUIRED =     22.77  INCHES       '     ""
  TOTAL  STAGES REQUIRED ASSUMING 2.30 INCHES  CARBON/STAGE = 9.90

"SPACE  VELOCITY -     3185.' 1/HR "        "      '.        "~~~ '.-.'•.
                                                            ;"   ,^, ^ , . '/ '

...PRESSURE OR.QP ACROSS. CARBQN._.=	11 .3_C_ INCHES H.2.Q     ... .... ' '.'  ',.  .
  PRESSURE DROP ACROSS PLATES =     5.69 INCHES H20
  TOTAL  PRESSURE DROP ACROSS STAGES =     17.08 INCHES H20



     RATE. EXPRESSION  USED IN DESIGN CALCULATIONS   ..   _ 			

  RATEC1 I ) = COEf-r t U-X( I I/XS)**A  * (YS02**ll|  * (Y02**O * (YH20**D)
     WHLKE  COEFMK *  EXP(-f./R» ( I/ ( T+460 )} I .	._		
          T=     200.
       -E/R-    5416.
          K=0.00033^
 0.38
1.000.
0.043
.0.480
                                                                  YH2()=
0.130
0.620
                                                   	0«._... 0.730
                                              134

-------
                APPENDIX A-8-3

WESTVACO MODEL BY MULTIPLE REGRESSION  (LOADING
FACTOR ORDER) COMPARED TO CONTINUOUS S02  SORBER
                Westvaco Model

  dXv
dXv     ,   -E/RT
-jrr  =  k e  ' ^
  where -E/RT = 5732°R

        A     =1.83

        n     = 0.53

        m     = 0.62

        p     = 0.73

        k     = 3.42(10"4)  gms.  H2S04/gm. C-min
                      135

-------
      S02 SORBER DESIGN

 RUN NUMBER     SA-21   DATE   6   7 71

_TOTAL CARBON RATE -   2.910 LBS/HR	
 OUTLET CARBON LOADING =  0.17885  LBS  ACID/LB CARBON
 HEIGHT Of- CARBON/STAGE =   2.?5  INCHES
 OIAItTER LT VESSLL •-=  6.0  INCHES	..._		
 CARBON USED "»  96324.
                            1247.  SCFH
                              _2009.  PPM
                                150.  PPM
                               0. 1300 ...... ...
                                  165.  PPM
 TOTAL GAS FLOW  RAFE  =
 INLET SO? CONCENTRATION  =
"INLET NO CONCENTRATION  «
 INLtT 02 VOLUME  F-RAC1IO.M =
 INLET H20 VOLUME  TRACTION *
 OUTLET S02 CONCEN1 RATION =

_TEHPfRATURC = ?00.0  F)FG.  F                  .     	„
            S02  CONCCNTRAT10N        ACID LOADING
     STAGE         PPM             LBS ACIO/LB CARBON
	   1    	   2009,  .		__ D«J7.8e	
        2           1840.                   0.1590
        3           1649.                   0.1367
        .4  		1436.	Q..U17.	
        5           1202.                   0.0843
        6            .951.                   0.0549
	7.__			692..	,	CW)24e>	
        8            443.                   0.0
        9            231.                   0.0
	0.41		165 ..0.001	0...0.	



 TOTAL CARBON REQUIRED -      21.17  INCHES
 TOTAL STAGES REQUIRED ASSUMING 2.25 INCHES CARBON/STAGE = 9.41

 SPACE VELOCITY  =     3600. 1/HR                   .      V  ;     .:                    ~

.PRESSURE DROP ACROSS CARBON.  =	10.5fa. I NCHES H20 ._..U;^11	.'....	__IL.^__			_
 PRESSURE DROP ACROSS PLATES  «=      5.29 INCHES H2U
 TOTAL PRESSURE UROP ACROSS STAGES  =    15.87 INCHES H20



.   .RATE EXPRESSION USED  IN DESIGN  CALCULATIONS	 		

 RATECIII=COEFF *  (1-XI I I/XS)**A *  (YSC2**B) * (Y02**C) *  (YH20**D>
.._ WHERE CDEFF--K. * CXPI-E/R* (1/J T.f 46QJJ J					

         T=     200.        XS=    0.38       Y02=   0.042      YH20=    0.130
	 -E/R=...  5732.  ...    .  .A=_.1.83JQ_	__	B=. . ..0.530			C=.   .0.620.     „  D=    0..730
         K=0.000342
                                              136

-------
       S02  SORBER DESIGN
                 SA-22    DATE   6 15 71
 RUN  NUMBER
_J.QT_AL  CAKBON RAT.E_ = .._3..260 LBS/HR			
 OUTLET  CARUON LOADING  *  0.22479 LbS ACIU/LB  CARBON
 HEIGHT  t:F CARBON/STAGE =   2.35 INCHES
_U1AKE.TER .OF.-.V.ESSE.L _= ._&c.0....1j " 6
'. • , 7
8
9
200.0 DEC, F
CONCENTRAT ION
PPM
3772.
3569.
... 3329,. . ..
3045.
2712.
2322,
1875.
1381.

ACID LOADING
LBS ACID/LB CARBON
0.2248
0.2082
0.1887
	 _ 	 0.1657
0.1386
0.1067 ' - '•' . ' •:'*: '•• - '• ": •"• '-a •;•<"
0.0694
0.0266
0.0
                                          	A..Q.	
  TOTAL  CARBON P.EQUIRCO =      22.24 INCHES
  TOTAL  STAGES REQUIRED ASSUMING 2.35 INCHES  CARBON/STAGE = 9.46
  SPACE  VELOCITY =
L_P_R£3SUG.E_DRQP_
                        3135.  1/HR
  PRESSURE  DROP ACROSS  PLATES  =
  TOTAL  PRESSURE DROP ACROSS' STAGES
                                     ,L,12 _LNCJiES__H2Q	
                                     5.56  INCHES H20
                                           16.68 INCHES H20
                          _LN. D.ES1G1.JLALCUIAT1UN.S. „
	RATt. EXPRESSION

  RAIECII ) = COE1:F *  (1-XI I )/XSI**A *  (YS02**B)  * (Y02**C> *  (YH20**D)
	WHERE CGtFF'K  *  EXP(-E/_R* I1/..I J_*46a»J I	.	™
          T*    200.
       TE/.R=.	-5Z32.
          K=0.000342
 XS=    0.38
...A?.._....»..6.3 0._..
                                                Y02=   0.042
                                              	B»_  0.530
                                                                  YH20=
                                                                           0.130
                                              137

-------
       $02  SORBER  DESIGN

 RUN NUMBER      SA-23   DATE  6 16 71

_!OTAL  CARBON  RATF  =   3.350 L9S/HR 	_„._
 OUTLET CARBON LOADING = 0.16660 LBS ACILVLB CARBON
 HEIGHT OF CARBON/STAGE =   2.40 INCHES
__UlAKETER  OF VESSEL =  .6.0.INCHES. 			
 CARBON USED =  96324.
 TOTAL  GAS FLOW RATE  -     1106. SCFH
.JNLET  S02 CONCENTRATION .=	2.0.0.9._. PPM	
 INLET  NC  CONCENTRATION -      150. PPM
 "INLET  02  VOLUME  FRACTION -  0.0420
 INLET  H2D VOLUME FR*CTI ON. .= __0...1.300.	
 OUTLET S(J2 CONCENTRATION ='       91."~PPM~

 TEMPERATURE  = 200.0  DEC.  F   _
            S0~2 CONCENTRATION         ACIO LOADING
     STAGE          PPM            LBS ACIO/LB CARBON
         I           2009._   _	_			  .0.1666	
         2            1764.                   0.1463
         3            1537.                   0.1240
   	4   	1,2.70..   	Q.0999	
         5             989.                   0.0745
         6             707.                   0.0491
	 _   7_	_4.42*,_      _  	0.0252.
         8             220.                   0.0051
     0.79         91.0000                  0.0
JTOTAL CARBON.  REQUI.R.EU_»
 TOTAL STAGES  REQUIRED  ASSUMING 2.40 INCHES CARBON/STAGE = 8.79

_.S_PACE: VELOCITY.? ____ 32J.4.  1/HR_ __________ ^ ______ , __ . _____ , ____ , __ ^

 PRESSURE DROP ACROSS CARBON  =     10.54 INCHES H20    :;  . •'.. ••••-. •;-•::
_P.RtSSURE DROP. ACROSS PLATES  =   __ S.^T^INCHES H20   ' ^'.'.f* ". '.  "
 TOTAL PRESSURE DROP ACROSS  STAGES =    15.82 INCHES H20
    RATE EXPRESSION USED  IN  DESIGN CALCULATIONS
 RATEC ( i - COE FF *  i i-x (  ) / xs > **A*  i vs2**B )  * ( v2**c  * "vH2o**o  '
    WHERE COEFF'-.K  *  EXP l-E/R« ( It I T + 460 I I )
          s    200.         XS=     o38        Y02=   o.042      VH20=   6.'l30 ...... ~     :
         R=   5732.          A=    1.830          B=   0.530         C=   0.620          0=   0.730
         K=0. 000342 ......... ________
                                              138

-------
       S02 SORBER DESIGN

  RUN  NUMBER     SA-24   DATE   6  16  71

 .TOTAL CARBON. RATE . = ._.?.. .190. LBS/HR	
  OUTLET  CARBON LOADING = 0.18034  LOS  ACIO/LB  CARBON
  HEIGHT  CF  CARBON/STAGE =   2.45  INC-HES
_OJAMETER. OF VLSSEL_»	6._0_1NCHLS	
  CARBON  USED =  9632'..
  TOTAL GAS  FLOW RATE =      965.  SCFH
_1 NLEJ__S02_CONC.ENJ_RAT [ ON «	3.982 ._PPH	
  INLET  NO CONCENTRATION =       150.  PPM
  INLET  02 VOLUME FRACTION =  0.0460
  INLET  H20 VOLUME. FRACT I_CN_=__0. 1_30_0_	
 "OUTLET S02 CONCENTRATION =      1078.  PPM
 JE.MPERATURE.; 250.0 OE6,_R	
S02
STAGE
„ 	 .JL.._ _
2
3
A ... '
5
6
7
8 .
9
10
11
0.04
CONCENTRATION ACID LOADING
PPM LBS ACID/LB CARBON
3982. 0.1883
3800.
3597.
3371.
3117.
2836.
2525.
, 2185.
1821.
1439.
1090.
1078.0002
0.1733
0.1565
0.1378
0.1168
0.0936 -:'.-:'' ; ' ••••'•' ' ' ' ::-- •••''•'
0.0679
0.0398
0.0096
0.0
0.0 : -• - '
0.0
,_JDJLAJL_CARBOS_R£ QU I RED. =.__ ___  ^_     ___________
j  TOTAL  STAGES REQUIRED ASSUMING  2.45  INCHES CARBON/STAGE =11.04
                        18Q .  1/HR
  PRESSURE DROP ACROSS CARBON =     13.52  INCHES H20
^_PAESSURE._ DROP-ACROSS . P.LATES_=	6.^.76_JNCHES_ H20		
I  TOTAL  PRESSURE DROP ACROSS Si AGES =     20.28  INCHES H20
     RATE  exPRESSIOM USED IN DESIGN CALCULATIONS
  RATl'C(I)»CUEFF * I l-X ( I )/XS) **A  *  **B)  *  IY02**C)  * (YH20**DI
     WHERE  COEFF-K *  tXPI-t/R»I I/IT + 4601I)
          T=    250.        XS=     0.38        Y02«   0.046      YH20=   0.130
       -E/R*   5732.         A*    1.830          B=   0.530         C=   0.620          0-    0.730
          X=0.000342	-'		..-_	—		-:	—		
                                              139

-------
       S02 SORBER DESIGN

  RUN NUMBER     SA-25   DATE  6  17 71

  TOTAL CARBON RAT f =  3.270 LBS/IIR
  OUTLET CARBON LOADING - 0.12817 LBS ACID/LB  CARBON
  HEIGHT OF CARBON/STAGE =   2.35 INCHES
  DIAMETER OF VESSEL =__6.0 INCHES	
 "CARBUN USED =  9f<324.
  TOTAL GAS FLOW RATE =     1094. SCFH
  INLtT S02 CONCENTRATION ^_   _2028. PPM   _     	
 "iNLtT NO CONCENTRATION""*'  ~" i so ."PPM	"
  INLET 0           .        '            \   :
_PBESSURE.'*DRPJ>_.ACROSS_CARBOri.=	11.61 INCHES H20
  PRESSURE DROP ACROSS PLATES -     5.80 INCHES H20
  TOTAL  PRESSURE DROP ACROSS' STAGES =    17.41 INCHES H20
     RATE .EXPRESSION USED IN DESIGN CALCULATIONS
  RATECII I = COEFF * I1-X(I I/XS)**A * (YS02**B) *  
-------
       S02 SOR6ER DESIGN

 RUN  NUMBER     SA-26    DATE  6  18  71

_TO.TAL .CARBON..RAJE..?_....3.,AOo.LBS^HR._	
 UUTLtT  CAROON LOADING  = 0.1852B LBS ACIO/LB CARBON
 HEIGHT  OF CARBON/STAGE =   2.30 INCHES
_DIAMETEK OF_VESSC.L. = _&,0._.U&. PPM_	
 INLET NO CONCENTRATION =      150. PPM
 INLEt 02 VOLUME FRACTION =  0.0430
_.INLE1 H20 VOLUME. FRAC.TICN_=	.0..13QO.....	
 OUTLET  Sl)2 CONCENTRATION -       46.  PPM

_TEMPERATURE =...200.0 DEC. f	   . 	_.
             S02 CONCENTRATION        ACID LOADING
      STAGE      ,    PPM             LBS  ACID/LB CARBON
                      2055,	 _ _Q_.1853
                      1879.                   0.1685
                      1685.                   0.1500
                                            _Q.,_1296
                                              0.1080
                                              0.0850
                                      '	Q»06.16._
                                              0.0390
                                              0.0186
   ,	10	IAD,           	_
  -.;•;   0.83          46.0000      ;    >:  :     0.0
  TOTAL CARBON REQUIRED =     24.92  INCHES
        .STAGED'KE.QU 1 RE0,AJSU.MJNfi,1-.3J)_'INCHE_S_ CARBOhi/STAGED?..lp..JJ_
  SPACE VELOCITY = -     2910. 1/HR
  PRESSURE DROP ACROSS  CARBON =     12.46  INCHES H20
  PRESSURE DROP ACROSS  PLATE.S =     6.23  INCHES H20
  TOJAL . PRESSURE. DROP AC.ROS,S_3JAG.E.S-. = .	18.69.. 1.NCHES....H20..,	
     RATE EXPRESSION  USED IN DESIGN CALCULATIONS

...RATEU I I-CQEFF *  < 1-X( I I/X$)**A.. * .(YS02**B)_Jf_ tYQ2**CJ.. *_t.YH2.0**D)		_	  	 	
     WHERE CQEFf:=K  *  EXPI-E/R* (I/ I T+460) ) )

	T»_	?JX>*	1_...  X.S.;	_0,.3.8...	V.Q2=	O.,0_43	YJ120*	0..1.30	
       -E/K'   5732.          A=   1.830          B-   0.530          C=   0.620          D=    0.730
          K=0.000342
                                              141

-------
                        APPENDIX A-9


             S02 SORBER DESIGN - EFFECTS ON SIZE
Appendix    A-9 includes the detailed results of the S02 sorber
design study which encompassed the effects of the following
parameters on reactor size:

     1)  Inlet S02 Cone.  -  2,000 PPM

     2)  Inlet 02 Cone.  -  0.046 mole fraction
     3)  Inlet H20 Cone.  -  0.13 mole fraction

     4)  Outlet Acid Loading on C  -  0.183 Ib. acid/lb. C

     5)  Temperature  -  200°F
     6)  Linear Gas Velocity  -  4 ft./sec.
     7)  Carbon Bed Depth/Stage  -  9 inches.


Each parameter was varied separately while holding all others
constant at the base conditions given in parameters in the
preceding list.

The results are summarized in Figures    A-9-1 to    A-9-10,
in which the dependence of reactor size on each parameter is
shown graphically.  Figure    A-9-1 shows the effect of inlet
S02 concentration on carbon requirement for a S02 removal of
90%, while Figure    A-9-2 presents the same effect but for a
specific outlet S02 concentration of 50 ppm.  All other cases
are based on a S02 removal of 90%.  Figures    A-9-3 through
   A-9-6 show the effects of 02 concentration, H20 concentra-
tion, outlet acid loading, and temperature.  Figure    A-9-7
shows the effect of linear velocity at carbon bed depths of 4,
9, 18 and 32 inches.   Figures    A-9-8 through    A-9-10 show
the effect of carbon bed depth at linear velocities of 2, 3,
and 4 ft./sec., respectively.

The raw results as obtained from the computer program are
presented following the figures.
                             142

-------
                  Figure A-9-1
Effect of inlet S0£  concentration on carbon required
to  remove 90%  of  the S02
00
                  -  40
                  •a
                  c
                  3
                  a-
                  &
O-
OJ
a


§
J2
10
•4J
O
                                                           Outlet Acid Loading:
                                                           Linea.- Gas Velocity:
                                                           Carbon Bed Depth/Stage:
                                                           Inlet Og Concentration:
                                                           Inlet HgO Concentration
                                                           Temperature:
                                           0.184 Ib. Acid/lb. Carbon
                                           4  Ft./Sec.
                                           9  Inches
                                           0.046 Volume Fraction
                                           0.13 Volume Fraction
                                           200° F
                                                     1500       2000        2500

                                                     Inlet S02 Con:entration, ppm
                                             3000
                                                                            3500
4000

-------
        Figure  A-9-2
                         Effect of inlet S0£  concentration on
                         carbon required to achieve  an  outlet
                         S02 concentration  of 50  ppm
   70
   60
 CO
   50
 OJ
 V-i
•H

 cr 40
4J
CX
0)
Q

a
O
30
4J
O
H
   20
   10
                                   Outlet Acid Loading:
                                   Linear Gas Velocity:
                                   Carbon Bed Depth/Stage:
                                   Inlet 02 Concentration:
                                   Inlet H20 Concentration:
                                   Temperature:
0.184 Ib. Acid/lb. Carbon
4 Ft./Sec.
9 Inches
0.046 Volume Fraction
0.13 Volume Fraction
200°F
              500       1000       1500      2000       2500

                                Inlet SOg Concentration, ppm
                                                          3000
            3500
4000
                                      144

-------
    Figure  A-9-3
Effect of inlet  02  concentration on
carbon required  to  remove  90% of an
inlet  S02 concentration of 2,000 ppm
   70
  60
  50
4)
.C
U
•o
c
   40
   30
a
4->
O
  20
  10
                   Outlet Acid Loading:
                   Linear Gas Velocity:
                   Carbon Bed Depth/Stage:
                   Inlet HgO Concentration:
                   Temperature:
                0.184 Ib. Acid/lb. Carbon
                4 Ft./Sec.
                9 Inches
                0.13 Volume Fraction
                200°F
              0.02
  0.04         0.06        0.08

  02 Concentration, Volume Fraction
0.10
0.12
                                  145

-------
       Figure A-9-4.   Effect  of  inlet  H£0  concentration  on
                          carbon  required  to remove  90%  of an
                          inlet S02  concentration of 2,000 ppm
   70
   60
   so
o
c
sr 40
5
o.
&   ,
§ '
•e
S30
                  Outlet Acid Loading:
                  Linear Gas Velocity:
                  Carbon Bed Depth/Stage:
                  Inlet 02 Concentration:
                  Temperature:
            0.184 1b. Acid/lb.  Carbon
            4 Ft./Sec.
            9 Inches
            0.046 Volume Fraction
            200°F
  20
  10
               0.04
0.08        0.12         0.16

H20 Concentration, Volume Fraction
                                                             0.20
0.24
                                    146

-------
      Figure A-9-5.
Effect of outlet acid  loading on
carbon required  to  remove  90% of
an  inlet  S02  concentration of
2,000  ppm
  140
  120
V)

u

* 100
 *
•a
   80
a.
£
   60
a
   40
   20
         Linear Gas Velocity:
         Carbon Bed Depth/Stage:
         Inlet 02 Concentration:
         Inlet HgO Concentration:
         Temperature:
4 Ft./Sec.
9 Inches
0.046 Volume Fraction
0.13 Volume Fraction
200°F
                                _L
             0.05      0.10      0.15      0.20       0.25

                       Outlet Add Loading, Ibs. Acid/lb. Carbon
                                 0.30
             0.35
                                    147

-------
     Figure A-9-6
         Effect of temperature  on carbon
         required  to  remove  90% of an inlet
         S02 concentration of  2,000  ppm
   90
   80
   70
VI

I  60
•o
2
   50
f!
o.
g

1  40
,2
   30
   20
   10
                  Carbon Bed Depth/Stage:
                  Outlet Acid Loading:
                  Linear Gas Velocity:
                  Inlet Og Concentration:
                  Inlet H20 Concentration:
                       9 Inches
                       0.184 Ib. Acid/lb.  Carbon
                       4 Ft./Sec.
                       0.046 Volume Fraction
                       0.13 Volume Fraction
     175
200
225          250

       Temperature, "F
275
300
325
                                    148

-------
      Figure  A-9-7
                    Effect of linear  gas velocity on

                    carbon required to  remove  90% of an

                    inlet SC>2 concentration of 2,000 ppm
                    at various carbon bed depths/stage
   80 -
   70 -
   60 -
VI
01

u
c
•o
OJ

•r-
3
cr

&
a*
o

•o

-------
               Figure A-9-8,
Effect  of  bed  depth on carbon required to remove  90%  of  an
inlet SC>2  concentration of 2,000  ppm  and  the  pressure drop
across  carbon  + plates
Ui
o
                 60
                •i
                •6
                t
                "5
               •5
               a.
               &

               S
               •e
                 40
                 30
                 20
                 10
                                                                                                               70
                                                                             60
                                                                                §
                                                                                •e
                                   Outlet Add Loading:
                                   Linear Gas Velocity:
                                   Inlet 02 Concentration:
                                   Inlet H£0 Concentration:
                                   Temperature:
                         0.184 Ib. Acid/lb. Carbon
                         2 Ft./Sec.
                         0.046 Volume Fraction
                         0.13 Volume Fraction
                         200° F
                                                                             40
                                                                             30
                                                                                                                  £
                                                                                                                  o.


                                                                                                                20o
                                              12
                     16
20
24
28
32
36
 10
40
                                                     Settled Bed Depth, inches

-------
Figure  A-9-9
Effect  of  bed  depth on carbon required to remove  9070 of  an
inlet S0£  concentration of 2,000  ppm  and  the  pressure drop
across  carbon  + plates
  60
 I
 u

 * 50
 £
 tx
 &
 o
 _ 30
 a
   20
   10
                                                                             60
                                                                               Si
                                                                             50.2
                                                                               t.
                                                                               3
                             Outlet Acid Loading:
                             Linear Gas Velocity:
                             Inlet 02 Concentration:
                             Inlet HgO Concentration:
                             Temperature:
0.184 Ib. Acid/lb,  Carbon
3 ft./sec.
0.046 Volume Fraction
0.13 Volume Fraction
200 °F
                                                                                                40
                                                                             30
           20?
                                                                             10
                               12        16        20        24

                                      Settled Bed Depth/Stage, inches
                                                28
         32
36
40

-------
           Figure A-9-10
hO
Effect  of bed depth  on  carbon required to remove  90%  of an
inlet S02 concentration of  2,000  ppm and  the  pressure drop
across  carbon + plates
                                                       Outlet Acid Loading:
                                                       Linear Gas Velocity:
                                                       Inlet Og Concentration:
                                                       Inlet H20 Concentration
                                                       Temperature:
                                           0.184 Ib. Acid/lb. Carbon
                                           4 Ft./Sec.
                                           0.046 Volume Fraction
                                           0.13 Volume Fraction
                                           200°F
            20
                                                   16       20       24

                                                 Settled Bed Depth/Stage, inches

-------
              APPENDIX A-9-1

EFFECT OF CARBON BED DEPTH/STAGE ON THE TOTAL
  CARBON BED DEPTH REQUIRED TO REMOVE 90% OF
   AN INLET S02 CONCENTRATION OF 2000 PPM
     Linear Gas Velocity,
     	ft. /sec .	    Run Number

               2               Test-1
               2               Test-27
               2               Test-28
               2               Test-29
               2               Test-30

               3               Test-3
               3               Test-31
               3               Test-32
               3               Test-33
               3               Test-34

               4               Test-4
               4               Test-5
               4               Test-6
               4               Test-7
               4               Test-8
               4               Test-9
               4               Test-10
               4               Test-11
                  153

-------
      S02 SORBER DESIGN

RUN  NUMBER    TEST-1    DATE   7 27 71

TOTAL CARUON RATE = 25.320 LBS/HR
OUTLET'CARBCN "LOAD ING =  6YT8375 ' LOSi""AC I D /'LB  CARBON
HEIGHT OF CARBON/STAGE  =    2.45 INCHES
D I AME TER OF V ES SE L_ =  18_.0_I_NCHES^__^	
CAR DON" USED""="  	~o>
TOTAL GAS FLOW RATE =      948'.. SCFH
INLET S02 CONCENTRATION^ 	_2..000* PP^	
"INLET 'NCTCON'CENTRAYlON  =  .~   T'50". PP'M: ; ;.• ••,''"•'•••}:;.*"!';"
INLET 02 VOLUME FRACTION  =  0.0460 ,   .;;   ::':  ;;" .:' •; :
INLET H20 VOLUME FR AC T I 0_N_=___0. 1_300_ -^ ^ '- ' '/j'v v--::j.
UUTLET"SU2 CONCENTRATION "=    """200 . "P"PM~ "~	
TEMPERATURE = 200.0  DF.G.  F	   	
	    S62'~CON'CENfRATTUN       "TcTO" LOAD ING'"*	
     STAGE         PPM    ,  .-.;:••"::.  LBS ACID/LB CARBON
        1  :          2000.-:-;>-:v:.'':.:;l'-::-::Xr::^:    -..'-0.1837
                     1723.                    0.1553
                                             0.1249
                                             0.0933
3
A
5
C
7
1426.
1117.
807.
511.
252.
                                             0.031?.
                                             0.0047
     0.23        200.0001                    0.0
TOTAL  CARBON REQUIRED  =      17.71 INCHES
TOTAL  STAGES REQUIRED  ASSUMING 2.45  INCHES;CARSON/STAGE  -:7.23
SPACE  VELOCITY =      3637.  1/HR
PRESSURE DROP ACROSS  CARBON .='.  ', : 8.86  INCHES H20
PRESSURE DROP ACROSS  PLATES, = :/•   4 .43;-INCHES H20
IUT_AL  PRESSURE DROP ACROSS .STAGES =;; :p3»28  INCHES H2o;
                               154

-------
     S02 SORBER  DESIGN
RUN NUMBER
               TESY-3   DATE   7  27  71
 TOTAL  CARBON RATE = 37. 98_0__L.BS/HR   __ ______
"OUTLET CARBOKfTbAUTNG" "="0". 1837b  LbS ACT07TB~CARB"ON~
 HEIGHT CF CARBON/STAGE =    I. 85  INCHES,
J31AMETER OF VESSEL =  18.0  INCHES _ ________ ____ _
 CARBON l"US"ED"= ..... ~" ..... 6."
 TOTAL  GAS FLOW RATE =     14227.  SCFH
 INLET  S02 CONCENTRATION = _  200p_. PPM
" I N L E f  N 0 " "CO N C EN T R A T 1 0 N ='" ~~~ ^"7l 5 : 0"."
 INLET  02 VOLUME FRACT ION  -  • 0.0460
 INLET  H20 VOLUME FRACTION  =  Q.I 300
 OUT LET 'SU"2~CONC"EN"firAnON "=
                                    "P P M"
                                    ___
                                 "200. PPM
TEMPERATURE  =  200.0 DEG. F
1- ;::: STAGE
2
3
4
•':.-.• "A1". iMv:1-:-' •:'. 6 X
^^OV^TH
8
9
10
: 11
: I i
;.--•: . • 12
S02 CONCENTRATION
::: :••,-- PPM
:iV; '"':^' '2000.
1858.
1711.
1558.
£'••£•' • I"--- .124*f*^.:w
920.
761.
607.
" ' £A 1 •:.:J!"'lv:::O
f O JL . : :,:.v.v:: :•:,...
ACID LOADING
LBS ACID/LB CARBON
0.1837
0.1692
0.1541
0.1385
:^%;.a :J:!*v,::;.:-i.;:.;-":.. ' 0. 1225 •..•.• -. v •.. . • • : ;.f ::;::i ;:,,-..-t
w4pps.f/:,;:>. . .'•. 0.1061 '". :-vi:::--:^: ••.^Sii^iJ,.-
'-:•, '•:•: .•:-.• •'•'•; *-.-' : :•: .•:•" ••;•' '-:-:•:•: ;.-••: .. __ ,,•.,•...•.••••.• - • •••.•.•>•-. .• •. .-• ;• • • •
.•:••.•;•:•• .• . : . . ; •:•.- •:• ;•:.,: f\ f\ (i G A - •• • ••• • • .-...-., :•• ••••• •* •• - - •- -
••.•••;; ' ' '•/ -.• • ••-•".-.' 	 •'-: - . -, • \j v \) o ^y o -:•' .-:•. . . • • , ' • ; : - "•:;:-••.-. :••-,• - :•.- •.-.'•
0.0731
0.0568
0.0410
On ~j A i '.''••• - •
* UC-O 1 .. ••.-...,... •:.•..•;..•.:
K:§ff::m. ^M ":. o .0122 " ' ""' v-^*f^:^:'.. • .
lii:;v;:i'^,;:;i^:;:::;'; ..; o . o . &&&:'•£**<'' '
    0.06
                 200.0001
0.0
TOTAL CARBON  REQUIRED  =      24.16 INCHES
TOTAL STAGES  REQUIRED  ASSUMING;;!.851.INCHE.S CARBON/STAGE  =13.06
SPACE VELOCITY  =
                      4000.  1/HR
PRESSURE""i3ROT"ACROSS  CARBON =  ;; 12.08 INCHES H20
PRESSURE DROP  ACROSS  PLATES =; 6.04 INCHES H20
TOTAL PRESSURE  DROP ACROSS STAGES = >;:v' 18.12  INCHES  H20
                             155

-------
      S02 SORBER DESIGN
 RUN NUMBER
              TEST-4
DATE  7 27 71
 TOTAL  CARBON RATE =__5^0_ IBS/HR	
"6 U T L E r C A R B 0 N ~ 10AD'ING = "6". 18 375 GTS" ACID*
 HfclGHT OF CARbON/STAGE =   1.65 INCHES
 DIAMETER OF VESSEL - 18.0 INCHES
"CARBON
 TOTAL
 INLET
 INLET
                                             CARBOf
       USED =      0.
      GAS FLOW RATE =    18969.  SCFH
      S02 CCNCFNTRATION_=_    2000. PPM
     "NOCCNCENTRATTO'N =
 INLET 02 VOLUME FRACTION =
 INLET 1120 VOLUME FRACTICN =
 OUTLET SO 2" CONCENTRATION "=
       150.
     0.0460
      0.1300
PPM"
                                200".  PPM'
TEMPJERATURE = 200 .0_ DEG._ F _
     	~'~S02~C'ONCE>yfRATION"
    STAGE         PPM
       I -:          2000.
                                     ACID  LOADING
                                  LBS ACID/LB  CARBON
                                           0.1837 ,
2
3
4
5
6
7
8
9
id
.:•:,.:••• '•• n
14
15
16
; 17 .
i " 0.86
1905.
1807.
1706.
1604., -.:;
1285.
1176.
1067.
958:. v;
850^-vP*
744.- :••::;>.
640.
539.
442.
351.
267.
200.0001
0.1740
0.1640
0.1537
'•h^mMt'f&i.Q'1'*!*- 	
0.1105
0.0993
0.0881
•^^m^:^--.:. '- 0.0770 , . . ••.:•;.• , . •', -: •:,..;.-, . ... -:;,
!;::$l;1^IS?':-;i;.;^ 0.0659 '', '
-------
      S02 SORBER DESIGN

 RUN  NUMBER    TEST-5   DATE   7  27  71

 TOTAL CARBON RATE = 50.640 JJ3S/HR
 0 U T L E T C AR BCN L0 AOTNG " = "0 .18 37 5~"L 8S~~ACTOTtFTARWfT
 HEIGHT OF CARBON/STAGE =   4.00 INCHES
 DIAMETER OF VESS_EL_ =  18_._0  INCHBS	"
"CARBONi""USED"=	     "0.    ~"   "           w
 TOTAL GAS FLOW RATE =     18969. SCFH
 INLET S02 CONCENTRATION =	  2000. PPM
 INLET NCTCUNCENTRAT ION"=" "    "T5
 INLET-02 VOLUME FRACTION =   0.0460
 INLET H20 VOLUME FRACTION ^   0.1300
"OUTLET S02r CONCENTRATTON =
TEHPERATUR
|:
I • STAGE
!v i
, 3
:"..: •-.-:.. '•'• :--'--' J;r':-;':
8
. ' * 0.56
i
,-_*_ 	 	 .,—.—.-,.•
E = 200.0 DEG. F
S02 CONCENTRATION ; ;
.PPM- •• '•4w:i*-:;v:
\2000..:::"Hiif:;i
1772.
1531.
1279.
;,:.: -:::X:'.:.:. 1023.
;.;->•;.;:• i;,V.. -.;,.768. '
..-'"-.'::'..:::,•':'. 525.
306.
200.0001

:. AC TO" LOAD ING " " ; -- 	 	
LBS ACID/LB CARBON . :
••:-..v:::xi. :V, :: 0. 1837 ;/' ..1: -f: '
0. 1604
0.1357
.0.1099
0.0836
0.0575
0.0326
0.0102
' 0.0
 TOTAL CARBON REQUIRED ^J^J^V. 22: INCHES^    _    	
"tCTAL STAGES REC07"RiEO ASSUMING "4.00  INCHES~CARBON/SrAGE

 SPACE VELOCITY =     3764.  1/HR
 PRESSURE  DROP ACROSS CARBON  -     17.11  INCHES H20
 P R E S S UR_1 J3R C l>_ ACR_OS S PLATES  =	8.56  INCHES H20	
'TOTAL  PRESSURE"DROP" ACROSS STAGES  =     25~.67~ INCHES H2o
                          157

-------
      S02 SCRBER DESIGN

 RUN NUMBER    TEST-6    DATE   7 27 71

 TCTAL CARBON RATE _= 50._6A_0 _L_BS/_H_R	
"OUTLET""CARBONLOADING V~0.~1.83T5 LBS ACID/LB CARBON"
 Ml: I GMT OF CARBON/STAGE  =    6.00 INCHES
 OIAPFTER OF VESSEL. =  18.0  INCHES ^^y^-/---^;^;:-^^. _
"CARBON" USED" = """   b.
 TOTAL GAS FLOW RATE =     18969. SCFH
 INLET S02 CONCENTRATION_=	2000. PPM
 INLET" NO" CONCENTRATION"~=   ~   f5bT PPM        '
 INLET 02 VOLUME FRACTION  ~  0.0460
 INLFT H20 VOLUME  FRACTION  -  •:, 0. I3QQ
~ OUTLET'~S02~CONCWTRA"fiW =      200."
$02" CONCENTRATION: M^rf. v ACID LOADING
STAGE PPM •:-:-x: M^iWilP;: LBS ACID/LB CARBON
'1 2000.:.pl||lli 0.1837
2 1663.
3 1299.
4 922.
*.-.. .••:•-.•• . •' 5 -• :.v;..;'-.-:;.: :..:' ••••;"' .-^•SSa.v^^-:;:::-::?.:::™*;1::'-^:::;-::-:::;-^:-.:-.?;-.^-,.
;-: .•: .• - . . •:-- ..-..J .-..-..•. :•-. ..•..--•. -•--; .:.....•.:-.... :•..-:• •* -»v •• ••.:-.-:-:•>.•:-:•::-:-:•:-:•:•:-::••:•:-:-:>:-.•:-•-:•/:•:•:•: :-::-r-Xv.- ,->.-,/:
;•• • .; . ' >v.v ;;. • - ; ;'•... <: ;.y -•:':' '.-x:' '• : • . : • : : ••-. • •• '• '-• • -:.:-. •• •-•• ' : •.; : -•:.x;.v<.:-:;:;:;:;1;1v:;:;:-'-> x-::>'-.-:- -:-1-'-:yX;>:-:-: .;:;••:< :• • •:••-
I^MCo'vi^l^r:';---^v2'ob;ooo'r:^II^M^K^.
0
0
0
i 0
:;.:0
;i-::0
. 1492
.1119
.0734
.0360 •:•.-. .. ;,:,:.,:-.-::•,, :.-,v..;::;;:,:-
.0035 •;;?;:• '^^•••^••^.'^•: v? :;'
. o .•::.;:-;" \i',:'r:'.x r^:K':':s-x::;':' ••''•....''.'??'."•
                              36.88 INCHES
TOTAL CARBON  REQUIRED =
TOTAL STAGES  REQUIRED ASSUM ING-. 6.00: INCHES  CARBON/STAGE =.,6.15
 SPACE VELOCITY =
                      3492. l/HR
                                          INCHES  H20
PRESSURE DROP _ACROSS_CARBON_f__	18.		
PRESSURE" "DRCP  ACROSS' PLATES =-\.:.j;-.. 9".22-."INCHES'"Hzo
TOTAL PRESSURE  DROP ACROSS STAGES =     27.66 INCHES H20
                            158

-------
      S02 SORBER DESIGN

 RUN NUMBER    TEST-7    DATE  7 27 71

 TOTAL CARBON RATE  =  50.64_p__LBS/HR
 OUTLET' CA'RBON"'LOADrNG~="0.183T5 ITS'" AC TBTLB~C/AR'BON""
 HEIGHT OF CARBON/STAGE =   9.00 INCHES  .vT  ,:  ;
 DIAMETER OF VESSEL = _ 18 . ?_I_N£HES      , ^:  : *:\:     V: :
"CARBON usEi>" =	---g^ ——   -.-    	  -~^   -
 TOTAL GAS FLOW RATE  =     18969. SCFH
 INLET S02 CCNCENTRAT10_N _=   	2000. PPM
 INLET NO COMCENTRAnON"= """"" ;  150. PPM"""'™     ~""~"
 INLET 02 VOLUME FRACTION =  0.0460     •   ;      ^
 INLET H20_y_CLUME  FRACTION  =. :-,0. 1_300A. x/!j"^£:;.?':"':-;-;:'
 OUTLET S02 CONCENTRAflbN =     ""200. PP~M~    ""

J§?lp-EMiyM_= 200.0_0_EG. F	
      	S02"CWc"ENfRAT10N        AC 10 Td'AD I"N"G
     STAGE     .     PPM             LBS ACIU/LB CARBON
        1           ..2000.                  °_«i83J_
                                            "0."1329
                                            0.0774
                                            r\
                      I -^ \S V                  • " "
    _____
2
3
4
1504. (
962. I
438. !
 TOTAL CARBON REQUIRED  =      40.76 INCHES
 TOTAL STAGES REQUIRED  ASSUMING 9.00 INCHES CARBON/STAGE = 4.J3

 SPACE VELOCITY =     3161.  1/HR
                                   20 . 3 8'
 PRESSURE DROP ACROSS  PLATES =    10.19  INCHES  H20
 TOTAL PRESSURE DROP ACROSS STAGES =     30.57  INCHES  H20
                           159

-------
      SQ2 SORBER DESIGN

 RUN NUMBER    TEST-8    DATE  7 27 71

 TOTAL CARBON RATE  = 50.640 LBS/HR             _   _
"6"UtLC"f™CARBON~LpA'0"lNG =' 0.113375 Lt5S AC 10/I5~CARSON
 HEIGHT OF CARBON/STAGE  =   12.00 INCHES
 0I A Y E T E R 0 F _ V E S S E L _f_JL8_.0_ INC HES 1               	
"CARI!UN"USEb "= 	~" 0.
 TOTAL GAS FLOW RATE =     18969..SCFH
 INLET SC2 CONCENTRATION =	_2009'_ p_p?l_      	  _
 INLHT NO CONCENTRATION"^	^  "" 1"50T PPM"  "   ""   ~~~
 1NLLT 02 VOLUME FRACTION  =  0.0't60
 INLCT H20 VOLUME F.RACTIGN_=	°JLJ^L?°_^	,	
"OUTLET S02~CG"NCENTRAnW~=~~     200. PPM

 TEMPERATURE = _200_.0 DEG_.  F		'	^_	
      """"    S02 CONCENfRAT'lO.N   ~^~   AX ID LOAD ING
     STAGE       V;   PPM             L6S ACID/LB CARBON
.:.. .  '  :  1' < :':'':'•:: :?:D;:;  ZOOO.                    0.1837  .  :
        2            1351.                    0.1173
        3             650.                    0.0454
     0.72        200.0001                    0.0
 TOTAL CARBON REQUIRED  =      44.67 INCHES
 TOTAL STAGES REQUIRED  ASSUMING12.00 INCHES  CARBON/STAGE = 3.72
 SPACE VELOCITY =      2884.  1/HR

 PRL"SSURE_DROP_ ACROSS  CARBON =    22.33  INCHES H20
'PRESSURE D'RO'P ~ACROSS"PLA"TES =    11.17  INCHES H20
 TOTAL PRESSURE DROP  ACROSS  STAGES =     33.50  INCHES H20
                               160

-------
      S02 SORBER DESIGN

 RUN NUMBER    TEST-9    CATE  7 27 71

 TOTAL CARBON RATE  =  50.640 LBS/HR
 OUTLET CARBON LOADING  =  0.18375 LBS ACID/LB  CARBON
 HEIGHT OF CARBON/STAGE =  18.00 INCHES
 DIA M E T IE R _OJ:_V E_SS_E_L_=_ 18.0 INC HE S   _____	
"CARBON 'USED ="     "  0.
 TOTAL GAS FLOW RATE =     18969. SCFH
 INLET S02 CONCENTRATION =	2000. ?P!t__	„_
 INLET "NCI"~CO'NCENtR"ATlON""=      I'JOi PPM:
 INLET 02 VOLUME  FRACTION =  0.0460
 INLET H20 yCLUME_ FRACTION =  0.1300	
"OUTLEt""S02" CCNCENTRATToN =      200". PPM

 TEMPERATURE = 200.0 DEG. F	    _
       	"~S02"CONCENT"RATl'ON '.: '-\ ";'•'''•  "AC I'D  LdAOiNG "~"
     STAGE          PPM        ':;::: LBS ACJD/LB CARBON
'  _    I.;"   .::;;. _, 2000.  :::/.:i:.V'i::i:x:>:.;v ...•:.   .0,^837..-..:
    "  "2            Y666.           "    .   0.0880
     0.93         200.0001                   0.0
 TOTAL CARBON REQUIRED:=  :.  .52.70 INCHES
TOTAL STAGES" REQUIRED  ASSUMING'IS.OO  INCHES  CARBON/STAGE = 2.93"
 SPACE VELOCITY =     2444. 1/HR
 PRESSURE DROP ACROSS  CARBON =    26.35  INCHES  H20
 PRESSURE DROP ACROSS  PLATES ='/•-'^ 13.17; INCHES  H2D	
TdfAL PRESSURE"DROP ACROSS STAGES =     39.52  INCHES H20
                              161

-------
      S02  SGRBER DESIGN

 RUN  NUMBER   TEST-10   DATE  7 27 71

JOTAL CARBON RATE  = 50.640 LBS/HR	   __
 UUTLbt CARSONT'OADING = 0". 13375 UBS ACID/LB CARBON
 HEIGHT OF CARBON/STAGE =  24.00 .INCHES
 DIAMETER  OF VESSEL = 18.0 INCHES
 CARBON  USED =      0.
 TOTAL  GAS  FLOW RATE =     18969.  SCFH
JNLET  SC2_CCNCENTRATIGN_=  	20_0_0_. _PPM
 INLET  NO" CONCENTRATION"^""	   rod. PPM
 INLET  02  VOLUME FRACTION =   0.0460
 INLET  H20  VCLUME FRACTION =  0.1300
 OUTLET  S02 CONCENTRATION *      200. PPM
S02
STAGE
. ' I
2
0.48
CONCENTRATION
PPM
2000.
808.
200.0001
ACID LOADING
L8S ACID/LB CARBON
0.1837 .../
0.0616
0.0
    A   C ARBON REQUI RED =     59.61 INCHES
                                                             __
       STAGES  REQUIRED ASSUMING. oo INCHES CARBON/STAGE = 2.48

 SPACE  VELOCITY = _ 2161.  i/HR
 PRESSURE  DROP  ACROSS CARBON -    29.81 INCHES H20
 PRESSURE  DROP  ACROSS PLATES = 	14.90 INCHES H2Q	
"TOTAL' PRESSURE DRQP'ACROS'S STA'GES~=    44.71 INCHES H20
                           162

-------
      S02 SORBER DESIGN
RUN NUMBER
              TEST-11    DATE  7 27 71
 TOTAL CARBON  UTE  =  50 . 6VOL B S/HR
                            _
"OUTLHT "CARBON LOADING  =  0.18375 Ll~S~~/rClWrB"Tfi"R'BflN~
 HEIGHT OF CARBON/STAGE =  32.00 INCHES :;•:/:•• v:.:::::::<.
 CARBON USED =       0.
 TOTAL GAS FLOW RATE  =     18969. SCFH
 INLET Sp2_CCNCE.NTRATION_= _^	2000. PPM
"INLET "NO"CCNC;ENTRAriON"--	    i~5b'."r~ppM"~~
 INLET 02 VOLUME FRACTION  =   0.04&0   ,,•'•'.••'
 INLET H20 yCLUME  FRACTICN =   0.1300_
 OUTLE T "502" CO'NCEN TR AT ION  =       200 .TP'M

 TEMPERATURE = POO.O  DEC.  F
            .$02.CONCENTRATION
     'STAGE         PPM
        (l            2000.
                                     ACID  LOADING  x..
                                  LBS  ACID/LB  CARBON
                                      • .•:*'.;;., ••-:. 0. 1837 •<"^
        2
     0.19
                     510.
                 200.0001
                               0.0311
                               0.0
 TOFALl
TOTAL
      CARBON
      STAGES
_REQU_I_R_ED'
 REQUIRED"
       70.10 INCHES
 SPACE VELOCITY =
 ASSUM1NG32.00INCHES  CARBON/STAGE = 2.19

1838. 1/HR
 PRESSURE DROP ACROSS  CARBON =
 PRESSURE DROP ACROSS  PLATES =
 TOTAL PRESSURE DROP  ACROSS STAGES -
                                  •35.05  INCHES H20
                                   17.52 INCHES H20	
                                        '52.57  INCHES H2"0"
                            163

-------
      502  SORBER DESIGN

 RUN  NUMBER   TEST-27   DATE  7 30 71

 TOTALL CARBON RATE = 25.320 LBS/HR          	   	
 OUTLET "CAR&'CNTbAD'iN'Gi = 6.18375 LUS ACID/LB CARETON
 HEIGHT OF CARBON/STAGE =   4.00 INCHES
                    = 18.0. INCHES
 CARBON USED =      0.
 TOTAL  GAS FLOW RATE =     9484. SCFH
 INLET_SC2_CONCENTRATION_f	2_P0.°_^ PPH.
""lNUET~N"C~CONCENTPrAfiON"- ..'-;.^-: "150". .PPM::-,"
 INLET  02 VOLUME FRACTION = ^(3.0460 :r-: W;:
 ^LE^J^O^ VOLUME FRACT I CN - ••:, :.Q. 1 300J-:.: f • ; !
"OUTLET su2" CCNCENTRA'TIUN =      200. PPM

 TEMPERATURE = 200.0 DEC. F
            S02 CONCENTRATION        ACID LOADING  ••
     STAGE         PPM            LBS ACID/LB CARBON.
        1    '        2000.                  0
2
3
4
1556.
1072.
S89.
0.1383
0.0887
0,0392
                 2 oo. ooo i^:;mmm$*m^ ^•^ ±o. o.
TOTAL  CARBON REQUIRED =     19.78 INCHES
TOTAL  STAGES REQUIRED ASSUMING 4.00 INCHES CARBON/STAGE  =  4.94

SPACE  VELOCITY.>     3257. 1/HR
 PRESSURE  DRCP ACROSS CARBCN =     9.89.INCHES H20
 PRESSURE  DROP ACROSS PLATES =     4.94 INCHES H20
 TOTAL  PRESSURE DROP ACROSS STAGES =    14.83  INCHES  H20
                            164

-------
     S02 SORBER  DESIGN

RUN NUMBER    TEST-28    DATE  7 30 71

TOTAL CARBON  RATE  = 25.320 LBS/HR
OUTLET CARBON  LOADING =  0.18375 LBS ACIO/L8 CARBON
HEIGHT OF CARBON/STAGE =   9.00 INCHES;
DIAMETER CF VESSEL:-  18.0 INCHES
CARBON USED =       0.
TCTAL GAS FLOW  RATE =      9484. SCFH
 NLET S2CCNCENTRATION        OO  PPM
         __ ___ _. _
"INLET NO "CONCENTRATION  =   ../;•• ispr PPM
INLET 02 VOLUME  FRACTION =  0.0460
INLET H20 VOLUME  FRACTION = ; 51 0.1 300
OUTLET S02 CONCENTRATION =       200. PPM

TEMPERATURE  =  200.0  DEG. F
           S02 CONCENTRATION        ACID LOADING
    STAGE   :       PPM            LBS ACID/LB CARBON
   ;:•:'" •;:l::::.r••-,•:• Ti:••v'w '2000.                  ..0.1837 •....
       2            1066.                   0.0880
    0.93         200.0001                   0.0
TOTAL taRBONREtR'EPOX:?
TOTAL STAGES REQUIRED  ASSUMING "9.00 "INCHES CARBON/STAGE  =  2".93

SPACE VELOCITY  - _ 2444.  I/HR             __ ........... __ _

PRESSURE DROP ACROSS  CARBON =    13.17 INCHES H20 ^^^§^51^
        -.-OROP- ACROSS .PES:-:^-:g^'::-:---6\' 5 9:. INCHES
TOTAL "PRESSURE DROP"  ACROSS STAGES =    19.76  INCHES H2o
                           165

-------
      S02 SORBER DESIGN
 RUN NUMBER
TEST-29   DATE   7  30  71
 TOTAL CARBON RATE = 25.320_LB$/HR  	 	
 CUTLET "CARBON" LOADING"'=~~"6 Vi aaYs TBS ACID/LB CARBON"
 HEIGHT OF CARBON/STAGE  =   18.00  INCHES,;;,;;
 DIAMETER OF VESSEL = 1.8.0  INCHES J'J*v£&*:/ii:
"CARBON'US'ED ------- o."~ "
 TOTAL GAS FLOW RATE =      9484.  SCFH
 INLET S02_ CCNCENTRATICN_=	2.00_0_._PPM
 INLET" NO" CONCENTRATION  =   "'  "150." PPM""
 INLET 02 VOLUME FRACTION =   0.0460
 INLET H20 V 0 L U K' E F R A C T I CN_  =  . 0. 13 00	
 OUTLET so2" CONCE"NTRAT"ION =       200. "PP"M~
I' "STAGE
\ .•••-. . 1.
0.10
:;';-:-..:/'.----. : PPM
•""'. ;':;'^.-;.'' .2000,
200.0001
ACID LOADING ,
IBS ACID/LB CARBON :-
0. 1837 x -:.>/
0.0181
0.0
 TOTA'L CARBON REQUIRED' -C y  37.83:-JNCHES  		
 TO"TAL STAGES REQUiRETASsuMiNl3l8.""oo INCHES CARBON/'STA'GE  =  2.10"
 SPACE  VELOCITY =
        1701.  1/HR
 PRESSURE DROP ACROSS CARBON  =
 PMSSURE_DROP__ACROSS_ PLATES  =   __
"ftiTAl"PRESSURE DROP"  ACROSS STAGES
                     18.93 INCHES H20
                      9.46 INCHES H20
                           28.39 INCHES H20"
                           166

-------
      S02 SORBER DESIGN

 RUN NUMBER   TEST-30   DATE  7 30 71

_TOTAL CARBON JATE = 25.320 LBS/HR	
 outLET~CAR'BON LOA'DiNG"'=" o"."i8375 "Cos ACi D/LB  cA'RBON"
 HEIGHT OF CARBON/STAGE =  32.00  INCHES
 DIAMETER Of VESSEL _f l8_.
-------
      S02 SORBER DESIGN

 RUN NUMBER   TEST-31   DATE  7 30  71

 TOTAL CARBON RATE = 37^9_80 LBS_/HR_
"OUt LET""CARBON ' LOADTNG" =. 0/10375  LBT'ATl ~07CB~~C'AR~BO"N
 HEIGHT OF CARBON/STAGE =   4.00  INCHES
 DIAMETER OF VESSELV;= 1^9_JLNCJjES	
 CARBON USED =	0."
 TCTAL GAS FLOW  RATE =    14227.  SCFH
 INLET S02 CONCENTRATION^	_?00.P_- PPM_
 INL E T "NtTCONC E N TR AT I ON =    ""  150T~ PP'M".,'
 INLET 02 VOLUME FRACTION =  0.0460       '
 INLET H20 VOLUME FRACTION ~  Q.I 300    •<
'OUTLET "S'02"CONCEN'tRATiON =       200.  P'PM
TEMPERATURE = 200.0 DEC. F
?.-"" .. " S02 CONCENTRATION
I STAGE : PPM
i V ••• 1 "'•' >:":. : 2000.
2 1699.
3 1376.
4 1040.
C " >;. ,; .' :: ' 0 . 7 5 I ? . i- . , v "' ; 2 0 0 . 0 0 0 .1;':; . :«; W^

: ACID LOADING
' LBS ACID/LB CARBON
... 0.1837
0.1529
0.1198
0.0854
.i. ••?:•• :.::••:??.•;• -x >;;•,-,..:-. -0.0512 . -..-;-::_ .••..:•:-.:•:
•£"#&&&:. :.:\ '.0 .0196 ::.^^i::\f ^.iv- -;;:-:
^kltSS^x?,0 * Q :?1 11^. v.:^: -₯'X\' '
 TOTAL'CARBON REQUIRED =     26.99  INCHES
 TOTAL STAGES REQUIRED ASSUMING 4.00  INCHES CARBON/STAGE - 6.75
 SPACE  VELOCITY =     3579. 1/HR

 PRESSURE  DROP ACROSS CARBON =     13.50  JNCHE_S H20	
 PRESSURE"'DRoFACRoss.PLATES =      6.75~rNCHES~"H20-
 TOTAL  PRESSURE DROP ACROSS STAGES  =     20.24 INCHES H2U
                           168

-------
       S02 SORBER  DESIGN

  RUN NUMBER    TEST-32   DATE  7 30 71

  TCTAL CARBON _RATE__^_37_. 980 LBS/HR
  OUTLET "CARBON "LOADING =  0. l8375"~LBS~
  HEIGHT OF CARBON/STAGE =   .9.00 INCHES:
  DIAMETER OF V ESSEL_= 18.0 INCHES
 "CARBON USED"=~~"  "   bT"
  TOTAL GAS FLOW  RATE =    14227. SCFH
  INLET S02 CONCENTRATION^  	  2A00- f?M
 "INLET W"CONCENTRATrdN>. " ...••.150.""PPM™
  INLET 02 VOLUME  FRACTION =  0.0^60
  INLET H20 VOLUME FRACTION - .0.1300
      "	SO 2" CONCENTRATro.N" =      20"6~.
 OUTLET
  TEMPERATURE =  200.0 DEC. F
  " "	" ~~ S02l'C 0 NC E N TR A T" I ON"
       STAGE     s;    PPM
  ;•'•-  •<:••:  i4l?i.tFi;f>:    2000.
         2
         3
      0.72
                                  " ~~"A"CTO~ro A D FN1S"	
                                   LBS  ACID/LB CARBON
                     650.
                 200t0001
OV1173
0.0454
0.0
  TCTAL CARBON  REQUIRED =     33.50 INCHES
  TOTAL STAGES  REQUIRED ASSUMING 9.00  INCHES  CARBON/STAGE = 3.72
C SPACE VELOCITY  =
                      2884.  1/HK
 PRESSURJLP_ROP ACROSS CARDQN  -
"PRESSURE DROP""ACROSS PLATES  =
 TOTAL  PRESSURE DROP ACROSS  STAGES  =
                                     6^75__I NCHES__H20	
                                     8.38  INCHES  H20
                                           25.13  INCHES H20
                               169

-------
      S02 SORBER DESIGN

 RUN NUMBER   TEST-33    DATE   7 30 71

 TOTAL CARBON RATE = 37.98p__L_BS_/HR __
 OUTLET" CARBON LO~A~DTNG'"=~0. 183~75 "LliS TCTD/LB  C'A~R"B~0~N
 HEIGHT OF CARBON/STAGE  =   18.00 INCHES
 C 1 AMCTER_ 0F_VESSEL «  18_. 0  1NCHES_^______	
'•CARBON USED "=      0."" ~
 TOTAL GAS FLOW RATE =     14227. .SCFH
 INLI:T SC2 CONCENTRAT I ON_=	2000. PPM	
"INLET NO ""CCNCENTR'ATION"*~     fso'T'ppM
 INLET 02 VOLUME FRACTION  =   0.0460
 INLET H20_ VOLUME FRACTION  =   0. 1300
'OUTLET "S02 CCNCENTRATION  =       200. PPM
ERATURE = <
S02
STAGE
1
2
0.48
?00.0 DEC. F
CONCENTRATION
PPM
2000.
808.
200.0001

ACID
LBS ACI


LOADING
D/LB CARBON
0.1837
0.0616
0.0
 TOTAL CARBON REQUIRED  = :: :   44.71 INCHES; ____ __ __ ___
       STT AGES' REQUrRED TSSUMINGIS.OO INCHES  CARBON/STAGK =
 SPACE VELOCITY =      2161.  l/HR
 PRESSURE DROP ACROSS  CARBON =:    22.36  INCHES  H20
 PR_ESSyRE_DRCP ACR_OSS_ PL AT_ES__=__ _^_1_1_._18 _INCHES  H20	
 "TOTAL" P"RESSUR"E"D"ROP'ACROSS STAG'ES =  "" 33753 TNCHE'S H2"o
                               170

-------
      S02 SORBER DESIGN

 RUN NUMBER   TEST-34    DATE   7 30 71

 TOTAL CARBON RATE = 37.980 j-BS/HR
"OUTLET"" CARBON TOADlNG = O.Tel 75 "LlS ACID/LB"~CAR"BON —
 HEIGHT CP CARBON/STAGE  = , 32 , 00 INCHES \           .:.
 DIAMETER OF VESSEL =  Ij.O INCHES ^/^.X&^Z"::-.'. :.'•: ': ."' ''..
             '    '~'~
 TOTAL GAS FLOW RATE =     14227.  SCFH
 INLET_S02 CONCENTRATION  =_ __  200p._P_P_M
 INLET NO "CCNCFNTR'AtiO'N "-"  "  "Tl50T PPM"
 INLET 02 VOLUME FRACTION =  0.0^60  .  ::
 INLET H20 VOLUME FkACTiqN_^ __ 0_. JL 3D 0_ £^_
 OUTLET $02 "CONCENTRAI 'ION" =      "200. "PPM
STAGE
1
2
0.00
S02 CONCENTRATION .':
PPM
2000.
204.
200.0001
ACID LOADING
LBS ACID/LB CARBON
0.1837
0.0
. 0.0
 TOTAL STAGES REQUIRED  ASSUMING32.00 INCHES CARBON/STAGt  =  2.00"

 SPACE VELOCITY =     1508.  1/HR
 PRESSURE DROP ACROSS CARBON  = ;• r:: :i'32.03'::INCHES H20
 PRESSURE DROP_ACRpSS_ PLATJES  =  Y  16 •« 02^ I NOME S H20	
TcfTAl PRESSURE"~DROP ACRCSS "SFAGES" =    48.o"5 INCHES H20
                             171

-------
                  APPENDIX A-9-2

EFFECT OF THE LINEAR GAS VELOCITY ON THE TOTAL CARBON
  BED DEPTH REQUIRED TO REMOVE 90% OF AN INLET S02
              CONCENTRATION OF 2000 PPM
       Carbon Bed Depth/Stage,
       	inches	     Run Number

                  4                  Test-27
                  4                  Test-31
                  4                  Test-5

                  9                  Test-28
                  9                  Test-32
                  9                  Test-7

                 18                  Test-29
                 18                  Test-33
                 18                  Test-9

                 32                  Test-30
                 32                  Test-34
                 32                  Test-11
                     172

-------
     S02 SOR&ER  DESIGN         •

RUN NUMBER     TEST-5   DATE   7 27  71
 TOTAL JDARBON RATE  =  5C	    	      	
""OUTLET CARB'CN TOADfNG = 6.1B37~5 LBS  A CID / L B CTfTBOlTTr
 HEIGHT OF CARBON/STAGE  =
JD IA M E TER _OF VESSEL = 18''.(
 CARBON USED =      0.
 TOTAL GAS FLOW RATE  =    18969. SCFH
J_NL.^T._1°1__C°.NCFIIRAJJ ON =      2000._ PPM  ___________
 I"NLET NO CCM^ENTR'At IO"N" = ..:,:: .,-, 150."  V9]^^:::<^:-.:^amK
.. INLET 02 VOLUME  FRACT ION := vifl '   '":'"':>™*--^>">• »--—-•—-
 INLET H20 VOLUME FRACTION  :=;::-.
"OUTLET~S02"CONCE"NTRA"Tro.N =

 TEMPERATURE = 200.0  DEC. F
                                  20 0. TPfi
|" S02
I STAGE
I , I 	
2
3
4 •
CONCENTRAT
PPM :/•;•;;;:••£
1772.
1531.
1279.
ION • -::v-x.:;v:::-::-.#- V AC 1 D . LOAD I NG >.i- v:^-:::.:*^-::;.- '•'*".
:;:|:::J|||g::;;.LBS AC 1 0/LB C ARBON: V/^^lf |i|«>'<:S>
0.1604
0.1357
0.1099
      56
                      306.
                 '200.0001
0.0102
0.0
TOTAL CARBON  REQUIRED >=?; ::.:; :: 34;22 JINCHES;
TCTAL STAGES  REQUIRED ASSUMING  4.00  INCHES CARbON/STAGE  =8.56
SPACE VELOCITY  =
                       3764. 1/HR
PRESSURE DROP  ACROSS CARBON; =
PRESSURE DROP  ACROSS PLATES =
TOTAL PRESSURE  DROP ACROSS STAGES  =
                                   17.11  INCHES H20 :5:»-»::«:i*-;₯V:V
                                    8.56;!::;INCHES H20^.:W:^	
                                          25.67 INCHES H20
                            173

-------
      S02 SORBER DESIGN

 RUN NUMBER    TEST-7   DATE  7 27 71

 TOTAL CARBO_N JUTE = 50.640 LBS/HR	
IJUTTETCARBON LOADING = 0.1837.5 LBS /
 HEIGHT OF CARBON/STAGE =   ;,9.00 INCHES
      ;TER OF VESSEL = is.o
_.
 CARBON USED =~     0.
 TOTAL GAS FLOW RATE =    18969. SCFH
  NLETS02 CNCENTRATION =     2000. PPM
 INLET" NO" CONCENTRATION -.  -:.;. ,,, 150.,PPM .
 INLET 02 VOLUME FRACT ION.,=:?; '0.0460;•wMiHl
. 1NLET_JJ20^VCLUME FRACTICiN ~ >.Q.
"OUTLET s"o2 CONCENTRATION =      200. PPM

 TEMPERATURE = 200.0 DEC. F
2
3
4
1504.
962.
438.-
0.1329 1
0.0774 /
0.0237
                 200,OOCl               -   0.0
 TOTAL CARBON REQUIRED =     40.76 INCHES
 TOTAL STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE = 4.53
 PRESSURE DROP ACROSS CARBON =    20.38  INCHES  H20
 PRESSURE DROP ACROSS PLATES -    10.19  INCHES  H20
 TOTAL PRESSURE DROP ACRCSS STAGES =     30.57  INCHES  H20
                           174

-------
       S02 SORBER  DESIGN

  RUN NUMBER     TEST-9   DATE  7.27  71
                                               .'- -. •  ' • •" -V
  TOTAL £ARBON  RATE  - 50.640 LBS/HR	  '_  	
 WTLET CARBaTTLOAblNG = 0.18375 ~LBS ACID/LB... CA~RBON
  HEIGHT OF CARBON/STAGE:=  18.00
  DIAMETER OF VESSEL =18.0 INCHES
  CARBON USED  =       0.
  TOTAL GAS  FLOW  RATE =    18969. SCFH
 JNJ-.ET__Sp2. P.CNCENTRATl ON =     2000. _____
  INLET NO  CONCENTRATION = .;;.:•;;,,. ISO. PPM   .
  INLET 02  VOLUME FRACTION - ;0.0460
  INLET H2p_VC_LUMC FRACTION = " 0.1300	
 'OUfLEf~S"02 CCNCENTRAT I ON =      200.  PPM
  TEMPEP.ATURE_= _200_^0 DEC. _F	
              S0~2  C 0 NC E NTR AT I ON aiiiif ^ >• AC 10 LCTAOING"
      STAGE          PPM        l|p:?:i,;BS;.ACID/LB .CARBON
          1            2000.     ^i^i^ili^iiiK?"'-b_»_l_837.'^''^
        f~~2  "~^*^~"    1066.                •   0.0880
      0.93         200.0001                 ^0»0
  'TOTAL STAGES  REQUIRED ASSUMINGIS.OO  INCHES  CARBON/STAGF. =  2.93
  x                                          ''  *
  SPACE VELOCITY  =     2444. 1/HR    .             	
w.   ,,
^PRESSURE  DROP  ACROSS CARBON =     26.35  INCHES H20
^PRESSURE  DROP  ACROSS PLATES =:::::?i 13.17  INCHES H20	
  TOTAL PRESSURE DROP ACROSS STAGES =     39.52 INCH'ES H20
                             175

-------
      S02  SORBER DESIGN


 RUN NUMBER   TEST-ll   DATE  7 27 71


 TOTAL CARBON RATE = 50.640 LBS/HR
"CARBO'N USED =      o.
 TOTAL GAS FLOW RATE =    18969. SCFH
_!NLET_SG2_CCNCENTRATION =     2000. PPM
~I"NLET~NO"CCNCEN"TR"ATION - ;.
 INLET 02 VOLUME FRACTION =
 INLET H20 VCLUME FRACTION^ V
"OUYLTT S02 CONCENTRATION =      200. PPM


 TEMPERATURE = 200.0 PEG. F

 TOTAL STAGES REQUIRE'!) ASSUMING32.00 INCHES CARBON/STAGE  =  2.19"


 SPACE VELOCITY =     1838.;l/HR
 TOTAL PRESSURE DROP ACROSS STAGES -    52.51  INCHES  H20
                            176

-------
       S02 SORBER DESIGN

  RUN NUMBER   TEST-27    DATE  7 30 71      ':'--.;?'oV'

  T(?TAL CARBON RAIL-  =25*320 LBS/HR	'	
 "OUTLET" CARBCN LOADING = 0.18375 UBS ACID7TO CARBW
  HEIGHT OF CARBON/STAGE-; •<: 4 „ 00 INC H E S, i. ^•^••. iAfe-':V!
  D IAMET V.R OF VESSEL • =  18.0 •' INCHES -i-' ^.:.}&%::&±>^&*-£
  CARBON' USED =       o.
  TOTAL GAS FLOW RATE =     9484. SCFH
  INLET _S02 CONCENTRATION _=	 _ 2000. PPM 	      __
 TNLET^NC CONCENTRATION^ :::;F 'T5"0.  PPM""
  INLET 02 VOLUME FRACTION =! 0.0460
 JNLET H20__VaLyME  FRACTION  -0.1300	
  OUT LET'S 02 C"CNCEN"fRATrD"N =      200". PPM

  TEMPERATURE = 200.0 OEG. F
           : ,:::::S02::CONCENTRATION;:?:.::J;:;:;l:::V ACID LOADING  • ,:
r:::^-:;;::^                              LBS ACID/LB CARBON:
^^M^fi''l&^;^lp^o'ob^:Pf::^P•  ,- .: .,   o.ios?.-:^
"   "     2          '  ll56^   "'^^      T^TT  571383
         3            1072.             ••-••'•'   0.0887
         4             589.               '    0
  TOTAL CARBON  REQUIRED =      19.78 I~NCHES
  TOTAL STAGES  REQUIREDASSUMING 4.00 INCHES CARBON/STAGE  = 4.94

  SPACE VELOCITY *      3257.  1/HR
  PRESSURE DRCP ACROSS  CARBON =     9.89 .INCHES H20
  PRESSURE DROP ACROSS  PLATES -     4.94 INCHES H20
  TOTAL PRESSURE  DROP  ACROSS STAGES =    14.83 INCHES  H20
                            177

-------
        S02  SORBER DESIGN              "

  RUN NUMBER    TEST-28    DATE  7.30 71

  IP™!- CARBON RATE = 25.320 LBS/HR
 1 U I M ^ ^* *S I '» L* V> I » I •* >~1 • l~    «_^w_*fc.** l».brvf---i              ^ ^         	
 TuTLET"C~ARBON LOADTNG = 0.18375  LBS AC 1D / L8  C AR BOlT.: .V ;:::,:.:,,;;:
 HEIGHT OF CARBON/STAGE =•• 9.00  JNCHE.S/:;;:^;;::^
 DIAMETER. CF VESSEL'' =.,18.0 INC^ESfe-fe^^                   **:?-vl
  CARBON US'EO =      0.
  TOTAL GAS  FLOW RATE =      9484. SCFH
  J NkEI__S°2  CC.NCEN'TRAT K1J1       2000. PPM
  "INLET NO CONCENTRATION  = ;.,;::^':;r,i5p.:..ppK~,	
  INLET 02 VOLUME' FRACTION  =^-^'^Q^bQ:;:^^^;^^i^^'-^-:^^. ||;f4
             yCLUME FR ACT I GN "-'::V-;'Q. Vsob;--^'-:^^                 f3g
             "CONCENfRATION  =      200.  PPM

  TEMPERATURE  =200.0 DEC.  F
S02
STAGE
i

2
0.93
CONCENTRATION
PPM
?000.

•'• 1066»
200.0001
ACID LOADING - •.;: .; ..-. :.<,.;&
LBS ACID/LB CARBON : : -v ;^i;::;
0.1837 :::"-s '•'•«':*:-•:••-•;

0.0880
' 0.0 _;.
..;,::•::::.;:>;.:
•\'.-:: •-:.•>-';! ::
....: .;:.::;:>:•. '•



  TOTAL STAGES  REQUIRED ASSUMING 9.00  INCHES- CARBON/STAGE =  2.93

  SPACE VELOCITY =     2444.  1/HR
'PRESSURE -DROP ACROSS
                                 ^W
                                         ::H.NCHEs-/H2o;:':--;;;;.:i:--:i-::t1|D^:l^
£':. PRESSURE  0R0P ACR0SS PL ATE'S>  -"---
                                            19.76  INCHES H20
TOTAL  PRESSURE DROP  ACROSS STAGES =
                            178

-------
      S02 SORBER DESIGN      -       -
                                  ' ''"*-.

 RUN NUMBER   TEST-29   DATE  7 30 71

              RATE = 25.320 LBS/HR
 OUTLET CARBON LOADING = 0.183~75 LBS  ACtD/LB  CARBON
 HEIGHT CF CARBON/STAGE; =  18.00 INCHES;;^;;.^:!^^^'-:
J)IAPETER_ CF VESSEL = . 18.0 . INCHESj^MflllB"'"	
 CARBON LIlTED = "     0.
 TOTAL GAS FLOW RATE =     9484. SCFH
 INLET S02 CCNCENTRATIQN =     2000.  PPM
                               150. PPM
 INLET  NO CONCENTRATION =   •:
 INLET  02 VClUME FRACTION =^
 INLET_ H20 VOLUME FRACTICN = ^,0>1300
"bUTlET S02 CONCENTRATION =
                                 200. PPM
 TEMPERATURE = 200.0 DEC. F
J STAGE
i • i
2
0.10
S02 .CONCENTRATION
PPM
e . 2000,
383.
200.0001
.ACID LOADING : . • SH: -;v./^:, .• •
iLBS AC I D/LB CAR&QU^rV-^^" ::'v
, ,, -• 0'k1837'^t^^is^V^-'.)V.
0.0181
0.0
 TOTAV'STA&ES REQUfRED ASSUM1NG18.00  INCHES CARBON/STAGE = 2". LO

 SPACE VELOCITY =	   1701. I'/hfR' =     -  -          	

 PRESSURE DROP ACROSS-CARBCN =
 PRESSURE DROP ACROSS PLATES":,-
                                  18.93
                                   9.46  INCHES.
 TOTAL PRESSURE DROP ACROSS STAGES =
                                        28.39  INCHES  H20
                            179

-------
        S02 SORBER DESIGN                 '.   .,  ... '    .

  RUN  NUMBER   TEST-30    DATE  7 30  71      ''.   -V"':-

  TOTAL CARBON RATE  = 25.320 LBS/HR	'
  ~OUtiL'ET"CARBCN LOADING = 0.18375  LBS  ACIO/LB CARBON
                           '                            "'
  HEIGHT OF CARBON/STAGE '-  32.00  i,,v,,,^- ,, ::,,::;:  ,,:.:;,::..   :,-.:
  _DI AKEY £R_0 F__VESSEL  ='"'18.0 .INCHES *::^^Mi%^^l^,-{i$?'Z
  CARBON USED =       0.
  TOTAL  GAS FLOW RATE  =      9484.  SCFH
  INLET_SC2 CCNCENTRAT10N  =2000.  PPM
  "TNLET  NO "CONCENTR'ATHTN" =  :•;:::;  -.156.: PPM..;•;;
  INLET  02 VOLUME FRACTION =-0.0460 i',:^'^
  _l N.LE.I  H20_yCL UME  FR AC T IC N_ =' '•••'<) ^ 1300 -y::;:;:-:!:
  bUT"LE"r'Sb2 CONCENTRATION =       200."~PPM.

  TEMPERATURE = 200.
        .:. ,,:.::,S02 CONCENTRATION         ACID LOADING
              •: . .,  ?iPPM             LBS ACID/LB CARBON
              ::  :  :^:.-V2000.                   0.1837
       0.67        200.0001                 .  0.0
t'-'TOTAL  CARBON 'RE"CUIRE'D.-.:;=S; #&5^
I0TOTAL  STAGES REQU IRED ASSUMING32..0,0 ...I.NCHES':: CARBON/STAGE =1.67:
  •*     '                               "  --'." * ' i  > .
  SPACE  VELOCITY =      1206. 1/HR           •-•.',
?.:•'• PRESSURE DROP ACROSS  CARBON.^^'•'•r. 26.71 INCHES  H20  ;,;,;;; :;;y;.,i:;.;
|:i PRESSURE DROP ACROSS  'PLATESf^ij1^ 13.36:;; INCHES  H20 '»''"$^i*?*;KJ
         PRESSURE DROP; ACROSS -STAGESl^^WiQl^.INCHES. H20-  g^ : x
                               180

-------
       S02 SORBER DESIGN          ,

  RUN NUMBER    TEST-31   DATE  7 30 71

  TOTAL_£ARB_ONI _RA_TE _~  37. 9130 I.BS/HR
 "OUTLET CARBON LOTOffiG =  0»l₯375 L₯
  HEIGHT OF CARBON/STAGE >••:   :4.00INCHES:
  DIAMETER OF VESjELs:- 1816.' INCHES?-;fi;:y;U^
  CARBON USED =       0.
  TCTAL GAS  FLOW  RATE =     14227. SCFH
  INLET Sp2_CONCENTRATiqNI_=_	 20°°' _pf.M
 "iNLET'NO CONCENTRATION = •...  .^1507 PPM"
  INLET 02 VOLUME  FRACTION <:x0.0460:i::H :.:"
  INLET H20  VOLUME  FRACTICN -""• 0.1300
  OUTLET "S02 CONCENT RATION"_ =      200. "PPM

  TEMPERATURE_=_200.0 DE_G_.__F	
             S02"CONCENTRATION  '  ~"AC ID  LOADING"
      .STAGE          PPM            LBS ACID/LB  CARBON
         1^	   2000..	0.1837 :M'^
     "   2            1699".    '               07T529
         3            1376.                  . 0.1198
         4            1040.                   0.0854	
     J^n^r^lll^:l»:C:',7p6',;:;;;:;; ^:isMii&M::'6.ObiYW^.
                 !?::;li?Mv.>.397'£::::::

   OTAL CARBON  REQUIRED .'<::-• .v^ 26.99:  INCH'ES .v
  TOTAL STAGES  REQUIRED ASSUMING 4.00  INCHES
  SPACE VELOCITY  =      3579. l/HR

 _P_RESSURE DROP ACROSS CARBON =    13.50  INCHES H20
" PRE:SSURE""OROP ACROSS PLATES = -^^ b.js • INCHES. H2ti: -/;,;,w^«.;
"•- TOTAL PRESSURE  DROP ACROSS: STAGESV=^.v^:!::70^24.>.INCHES;-H2g:WI:ij
                              181

-------
      $02 SORBER DESIGN

 RUN NUMBER   TEST-32    DATE  7 30 71
 TCTAL CARBON R.AJJ_=_AI^.M5 J^M/Jl?. __
"OUTCEfCARBON LOADING  -~:" 0 .1 8 3 7 5 L6S  ACTp/LB
'  OUTl ET'CARBON  LOADING ~":" 0 »18 3 7 5  L6S .ACTp/LB"CAR00"N  ...  ..,-...; s::UV •.'.:.;,;
  HEIGHT OF CARBON/STAGE = -••.9.'00 .l^ES^^;^^^^-^?.^}-^^^^
^_DIAKETER_ 0F • V ESSE L• • - -,' 18 . 0 •'I NC'HE S ;::::.;;:gg;|||g||||i|g
  rADUfiK»iicPn=       n.
 CAR13UN USED =       0.
 TCTAL GAS FLOW RATE  =     K227. SCFH
 JNLET S02 CONCENTRATION  =     2000. PPM
"rNLE"t"NO'~C6NCENTRATlON =   ,:> i'.JLSO. ;PPM .j.
 INLET 02 VOLUME FRACTION —.'v
 INLET H2p__yj]LUME  FRACTION -T	
"onuYLErsoT"l;"o'NcTNrRATroN~=      200. PPM

 TEMPERATURE = 200.0  DCG» F
            ..... S 0 2 .. C 0 NC E N TR A T I'D N.J-;- .:. •! >f C iixl % : A CTD LOADTNG
            --^^^^^^
                                                CARBON ':;-:"''':^::'^iii|li!^
                         V^Si^
        2             351.                    0.1173
        3             650.                    0.0^54
     0.72        200.0001                   ' 0.0
 TCTAL CARBON REQUIRED  =      33.50  INCHES
 TOTAL STAGES REQUIRED  ASSUMING 9.00  INCHES  CARBON/(ST«GE  =  3.72

      ~               ?e 84 .  i /HR ' !^^^^mf&n^£^^^-2-^f^^^^m
 PRESSURE DROP_ACRGSS        _
'PRESSURE DROP ACROSS' PLATES =     8.38  fNCHES H20
 TOTAL PRESSURE DROP  ACROSS STAGES =  .   25«13 INCHES H20
                           182

-------
      S02 SORBER DESIGN

 RUN NUMBER   TEST-33    DATE   7 30 71

 TOTAL CARBON__RAYE ^37.980 LBS/HR
"OUTLET "CARBON LO AIDING = 0.18375 TBS
 HEIGHT OF CARBON/STAGE.=  18.00 INCHES:
 C IAMETER OF VESSEL... - . 18.0  INCHES-;:::-::::.-.-.-.>H^M^^^I^
 .     .                             _ _
"CARBON USED =      0.
 TOTAL GAS FLOW RATE =     14227.  SCFH
 I NL E T_ S C <1_CONC E N T R A T I ON  = ___ 2 OOP. P P M
"rNL'Et NC" CONCENT RA'TTON =::,.;.  ' 150.. PPM
 INLET 02 VOLUME FRAC.T ION •=: 0.0^60
INLET H20 VOLUME  TRACTION --
OUTLET S02 ~f.C~NCENTRATl6'N =

TEMPERATURE_=^_2p_0.0  DEGJL_F	
           SU2,CONCENTRATION.
    STAGE
       r
                               0. 1300
                                  200. PPM
                                  •::x ••::•: AC I D • L0ADI NC'•."-':: -j
                                   LaS ACID/LB CARBON
                                            0.1837 :::
        2
     0.48
                     808.
                 200.0001
0.0616
0.0
"TOfAL STAGES REQAHRED  ASSUMING18.00 INCHES CARBON/STAGE = 2.4T

 SPACE.VELOCITY =     2161 c  i/HR
 PRESSURE
 PRESSURE _. ^	^_	,      	_.
 TOTAL PRESSUfiiE DROP  ACROSS STAGES -    33.53  INCHES  H20
                              183

-------
      S02 SORDER DESIGN

 RUN NUMBER   TESY-34   GATE   7  30 71

 TOTAL CARBON JA_TE = 37.980 LDS/HR	
~CUTL£f"CAR80N LOADING = 0.18375 LUS AC1D/LB CARBOTT
 HEIGHT Or CARBON/STAGE =  32.00 INCHES..>•;....^::«:-::4':;,:u:ij|>
 DIAMETER CF VESSEL =  18.0 INCHES :.. ry^iXBijiffiV:U^li^.
'CARBON USED =      o.
 TOTAL GAS FLOW RATE =     14227.  SCFH
 INLET SO? CONCENTRATION =	2000.  PPM
TNLET" NO" CONCENTRATION' =   ;: .. :150".  PPM,.:.:.;::
 INLET 02 VOLUME FRACTION  = r 0,0 4 6 0 :^'^&f;
 INLET H20 VOLUME FRACTION =; V0.1300
OUTLET S02 CONCENTRATION^ 200. PPM
TEMPERATURE •- 200.0 DEC. F
STAGE
2
o.co
S02 CONCENTRAT ION ;;::i:;: : y:
pp^'-^KM^M^s
204.
200 ..rtnni

/::.ACID LOADING ,,; ;.' ':.,. •:;£;$&&• v: -A:
ISVAC'ID/LB CARBON ."V: •••₯^-j^S\^,
ilSIIO '0.1837: -v, '••• ; ':^*9#£%$$.?%
0.0
. 0.0
 TOTAL CARBON RECUIRED;•'-.%•••;•• ,:.:V64.07 :INCHES'•".•^^••^
 TOTAL STAGES REQUIRED ASSUMING32.00 INCHES CARBON/STAGt = 2.00

 SPACE VELOCITY =     X508.  1/HR
 PRESSURE DROP ACROSS CARBON  =     32.03 INCHES H?.Q
 PRESSURE DROP ACROSS PLATES  -:  :" i ISiO^VkNCHES H2(f
 TOTAL PRESSURE DROP ACROSS  STAGES -    ^8«OS  INCHES  H20
                            184

-------
                   APPENDIX A-9-3

EFFECT OF THE INLET 02 CONCENTRATION ON THE TOTAL CARBON
    BED DEPTH.REQUIRED TO REMOVE 90% OF AN INLET S02
                CONCENTRATION OF 2000 PPM
                             185

-------
       S02 SORBER DESIGN

  RUN NUMBER    TEST-7   DATE  7  27  71          .

  TOTAL CARBON RATE = 50.640 LBS/HR	_      _    "	
 ~bUTrET"CAR"BWTOADING = 0.1837.5 IBS  AC IJD/LQ CARBON" ..".,;.,i...:;.;..., .v.......,:;.. ,
  HEIGHT OF CARBON/STAGE > -.;C:..9.00' INCHES  '^MKiif^&^^fQ^M^^y
 _PlA-NEJLIB. _OF VESSEL = 18.0; INCHES   . .; .  .  ffxrlfe;;^
 TA'RBON USED =     "o.
  TOTAL GAS FLOW RATE =     18969.,  SCFH
  INLET S02 CONCENTRATION =	2000.  PPM
  INLET 02 VOLUME FRACTION =  . . ^0 . 0 A 6 0
   .   __
  OUTLET  S02" CONCENTRATION
  TEMPERATURE = 200.0 PEG. F
         2   "       1504.                   0.1329
         3            962.                   0*0774.
         4            -'tjC.                   O.G237
  TOTAL CARBON REQUIRED =     40.76  .INCHES
  TOTAL STAGES REQUIRED ASSUMING  9.00 INCHES CARBON/STAGE = 4.53
^: :S P AC E' VELCC IT YH='f:: ;-^
  PRESSURE DROP ACROSS CARBON  -     20.38 INCHES H20
  PRESSURE DROP ACROSS PLATES  =     10.19 INCHES H20
  TOTAL PRESSURE DROP ACRCSS STAGES =    30.57 INCHES  H20
                              186

-------
       S02  SORBER DESIGN

  RUN NUMBER    TEST-12   DATE   7  27  71

  TOTAL  CARBON RATE = 50.640 LBS/IIR
  'CUTLET  CARBON LOAOfNG"'=" O'.'l 037fi" L TiS ~AC IDYCTfCARBON"
  HEIGHT  OF CARBON/STAGE =   0.00 INCHES
  DIAMETER  OF  VESSEL ~  1_8»0  INCHES   _ i __i __
  CAR BUM  USED  -      67 	"~"'          "~
  TOTAL  GAS FLOW RATE =     HJ969. SCFH
  INLET  S02 CONCENTRATION =    _ 2000.  PPM _
  INLET  NO  CONCENTRATION^	"~" ~150'.~P'N"",~. 3""~
  INLET  02  VOLUME FRACTION  =   0.0200 :; .;>:: ::      •
  INLET  H20 VOLUME FRACTICN  ^..^l-iOp,    ; ________
  "OUTLET  s'o'2  CONCENTRATi'dN""= "   " 20b.~"pp~M

  TEMPERATURE  = 200.0 DEC.  F
              S02. CONCENTRATION  ,       ACID LOADING  ~'
      STAGE          PPM :  ::::,:;• ;:;'';:    LBS ACID/LB CARBON
            "                ':^^--^^--:'.. ^..  o.
&' _iii'- ;^^ i.1^^. Uu_.   •••-_•
          2            1699.                   0.1530
          3            1377.                   0.1199
          4            1041.                   0.0855

  TOTAL  CARBON REQUIRED =   '•   60.80  INCHES
  TOTAL  ST'AGES REQUIRED ASSUMING  9.00 .INCHES CARBON/STAGE  =  6.76
         VELGC I  Y       2l9.

  PRESSURE  DROP A C R 0 S S C A R B ON =     30. 4 0 INC H E S H2 0 __  m_
  "PRESSURE"  DROP" "ACROSS "PTAT"ES""="    15.20 INCHES H20
  TOTAL  PRESSURE DRCP ACROSS STAGC-S =     45.60 INCHES  H20
                             187

-------
      S02 SORBER DESIGN
 RUN NUMBER
TEST-13   DATE  7 27  71
 TOTAL CARBON RAJEjf_ 50.640 JJISVHR	
~ffUfL'Ef""CA"RB6N""LOAOINe""=""oTl8375  IBS  ACTDTLB CARBW
 HEIGHT OF CARBON/STAGE =    9.00  INCHES
_D I A ME T ER_ C F_V E S S E L JL 19 . P_J.NCHE_S__	,	
 CARBON USED =      0." """
 TOTAL GAS FLOW RATE =     18969.  SCFH
 INLET S02 CCNCENTRATICN_ =	2000.  PPM	
""INLET" NO"CONCENTRATION""=       1~50T"~	"
 INLET 02 VOLUME FRACTION  =•  0.0300
 INLET H20_VCLUME FRACTION =0.1300
"OUTLET S02~ CONC'ENTR'AT'TON"*      "200T
                       PPM
                         PPM
STAGE:
!•>••;•'
2
3
4
••.,-• "-,5v.-;-
^/•v0.53;:-.-,v:
S02 CONCENTRATION
PPM
-.:! .2000.
1616.
1199.
773.
:. -:.V:,-:-. »- -•• 378. .:-:-::/:
•;•-:- 2 oo. ooo i M-S
ACID LOADING ^
LBS ACID/LB CARBON :;
0.1837 '".. ••••'; •. ..;,,..:
0.144A
0.1017
0.0580
mm^, ::::c;,, .••. o.or/6.,.^._,-::.-.. ........
WZSvtst. i.:;: :?*;:*%*£ Jv 0.0 ••••• ''• ^-'••- • ' •'• 'A^:- K-S'* '•> '••»' ••'••' ••••'"•
myV!-ffiKX^M;Vf
-------
      S02 SORBER DESIGN

 RUN NUMBER   TEST-14   DATE   7  27  71

 !PJ"AL C.AR!i.ON_RA-lE "... 50*640 LBS/HR   	
"OUT"L"ET~C"A"R₯ON""LOAOING =;  o. r83"75~TB~s~ AC 1 D/FBTARBON"""
 HEIGHT OF CARBON/STAGE =   9.00 INCHES
_D IAMETER_ eF_Vj[SSE L  =  18.0  INCHES  '	
 CARBON~usED =   	   o.
 TOTAL GAS FLOW  RATE =     18969.  SCFH
 INLET S02 CONCENTRATION^ __2000. PPM
"INLET"NCTCONCENTRATTON" =  "  " i"5C)7
 INLET 02 VOLUME FRACTION  =   0.0600
 INLET H20 VCLUME FR_AC_TICN =   0.1300
 OUTLET "S02" CCNC'ENTRA'T i'0'N "= "    200 .
TEI*
f:-;--. •-.'.'

|- :,.- ••;.
1PERATUR
STAGE
•:,;• . l>
2
3
4
0.05
,E = 200.0 DEC. F
S02 .CONCENTRATION
PPM
2000.
1419.
788.
223.
:..::: 200.0001 :Vx:;:::::v-::

ACID LOADING : ;
LBS ACID/LB CARBON ' ;V
o. 1837 . . .;•;•••• .;.''"..; ;.:-{'.-K:
0.1243
0.0595
0.0017
:.:.::•::.'., •..-^•••- ::;...: ;.. 0.0 .. .' . . .:f:; ;;:
 TOTAL CARBON REQUIRED =      36.42  INCHES
 TOTAL STAGES REQUIRED ASSUMING  9.00 INCHES CAR B3N/ STAGE = 4. 05
SPACE VELOCITY,*
                      3537.  1/HR
 PRESSURE DROP ACROSS CARBON  *     18.21  INCHES H20
 PRESSURE DROP ACROSS PLATES  •      9.11  INCHES H20
 TOTAL PRESSURE DRO.P ACROSS STAGES  »     27.32 INCHES H20
                            189

-------
      S02  SORBER DESIGN

RUN  NUMBER   TEST-15   DATE  7 27  71

TOTAL CARBON RATE = 50^640 LBS/HR_
'CUTLET ' CAR'NCN LOA'D1'NG~ = " 6 . 1 8 3 7 5""L JJS~7kin'TJ7 L B . CWfl'ON""
HEIGHT OF CARBON/STAGE =   9.00  INCHES
DIAMETER  U F  V E S S E L = 18 OWCHES
CARBON
TOTAL
INLET
INLET
INLET
INLET
OUTLET
USED = 0.
GAS FLOW RATE =
S02 CONCENTRATION =
NO CONCENTRATION =
02 VOLUME FRACTION
H20 VOLUME FRACTION
S02 CONCENTRATION
18969
= 0.
=
. SCFH
2000. PPM
1000 •:,;;: 'v:';:;-':i; :•';>••:; • ...
200. PPM
 TEMPERATURE = 200.0 DEG. F
i; STAGE
!• " ' :•••;• 1
2
3
0.2»
S02 COivCr-NTRATlOM
PPM
2000.
1220.
403.
200.0001
ACID LOADING
LBS ACIO/LB CARBON
0.1837
0. 1039
0.0201
0.0
 TOTAL  CARBON REQUIRED =     29.51  INCHES
 TOTAL  STAGES REQUIRED ASSUMING 9.00  INCHES CARBON/STAGE =  3.28
 SPACE  VELOCITY =     ^365. 1/HR

J?.RE_SSyRE_DROP ACROSS CARBON - ::    14.76  I NCHES_^H20_	
 PRESYUR~£  DROP'TCROSS PLATES =    " 7.38"""l"NCHE"S H20
 TOTAL  PRESSURE DROP ACROSS STAGES  =     22.13 INCHES H20
                            190

-------
                 APPENDIX A-9-4

EFFECT OF THE INLET H20 CONCENTRATION ON THE TOTAL
CARBON BED DEPTH REQUIRED TO REMOVE 90% OF AN INLET
           S02 CONCENTRATION OF 2000 PPM
                     191

-------
      S02 SORBER DESIGN               .

 RUN NUMBER    TEST-7   DATE  7 27  71

 TOTAL CARBON RATE = 50.640 LBS/HR	
T)UTrErcTRBON"TnA€ING =. 0.1837.5.-.LBS  AC I D/.LB CARBON
 HE IGHT 'OF CARBON/ STAGE *  '
•DIAMETER OF VESSEL '= 18 .0
 CARBON USED =      0.
 TOTAL GAS FLOW RATE =     18969. SCFH
 INLET S02 CONCENTRATION =	2000. PPM
 INLET NO CONCENTRATION -.
                               '150.
 INLET 02 VOLUME FRACT ION . =l:;.OV0460-i!^^|;|||i§|||g^^
 INLET H20 VCLUME FRACTION =:,::>:• 0i" 130&iK^jSM^MMJm
"OUTLET 502 CONCENTRATION =
 TEMPERATURE = 200.0 DEC. F
                                 200.  PPM
            .502 CONCENTRATION.
                                      ACID  LOADING
     0.53:Ma:.::.::.U:200.0GOI
                                        ;:;;;.;:-::| ;.0.0.j:g
STAGE
1
2
3
4
PPM
2000.
1504.
962.
LBS ACID/LB CARBON ^^Xtf*^ '" -:•
:;-v:V:'.: - 0.1837 •••'••'' :: ''•'''"'?'' :*-"'A:S-:V. :.••••"'
	 . ,. -:'-v';V ."•»«-'• -::.-.;,• ••..-.•:.:•. v':- ::' • •-'.—.-"
0.1329
0.0774
0.0237
 TOTAL CARBON REQUIRED =     40.76  INCHES
 TOTAL STAGES REQUIRED ASSUMING 9.00  INCHES CARBON/STAGE = 4.53
;.;.; ...;•.'.;•• ::.-; •••';; •y^-'.ViY
SPACE VELCC
•;:.:-. . •/•. ;- : .-•;•>-.;..;..• ,:
• . . • .••• ••-: •• • -•-•..
.•'.-. •''•;-.';'.'.• ••'.'..'.•'.•,•.•.:•:-'.'.•;•' .'.-..','.•.•' .".'
:TY:..= --':'--:;:'iK3l6'ii'
•' ••v-.V/'ir i:.--'-: V' J:?:::W::.:^:::!':';"::''' •-.•:".
	 .••••--•••• . -• • ••.-••-•-• •-•••:.•.•:-••.
:;:J:s:.':;s:?;
•1/HR:

•:-::';:-:•::;:••'•••••:
;|;|?;::;s.;;:|::.v.
;;;x:;;;;-.;::.j:i:?S;j;2x
.':'.•'':'£"'•' '.•'.'?'''x'x':'.
:';:•:-::: ••'•:. .;::•>:••:••
f&:-V£tifK
ii:₯Siffii-i£:!-i?::;%
Jiiggi:;; •:':"»:
•'•. •! .-"•, '•':'- ' '•'• '•.
£^&&£?g$*.^t
;-;:.;i;:.:.::::;: ^;^3x££'& ^^l
;>:;:>:•>. ';V'1::'".:;v;:''';::'"':'OX''::::;:;':-t':*
•'•' •; -•'•- ••'•':';-'/-.:.:v ;':••.' •::.:;'•-;'•'•:•:•
:-X':-.-
•:•;•:•>
;''|;';| •
'•: >::::
<:,•:•: :'.\-..>
--•.;-;•>:: •:.:-• v
•"^*S**:
••; •:':•• :-':: •
 PRESSURE DROP ACROSS CARBON =     20.38  INCHES H20
 PRESSURE DROP ACROSS PLATES =     10.19  INCHES h20
 TOTAL PRESSURE DROP ACRCSS STAGES =     30.57 INCHES H20
                           192

-------
       S02  SORBER DESIGN

  RUN NUMBER    TEST-19   DATE   7 27 71

  TOTAL CARBON  RATE = 50._640_LBS/HR_  _  _  _
  OUTLET CARBON i TOADTNG "=  0.18375 LBS ACT07FB"*"CARBON
  HtlGHT OF CARBON/STAGE =   9.00 INCHES
  PIAAET_?.?  °.f. VESSEL = IB. 0  INCHES          _____
 ""S'EO"=""~ "  0.         ~~"
  TOTAL GAS  FLOW RATE =     18969.  5CFH
  INLET S02  CONCENTRATION  =      2000. PPM
  INLET NO  CONCENTRATION  =       150. PPM
  INLET 02  VOLUME FRACTION  =   0.0460 ^  .: :  . ,. ,•:     .  . ;•;
  INLET H20 VCLUME FRACTJ CN =   0.1000 :;;^   ,_;•:;,. \..^_ •,
  "OUTLET"S02" CbNCENtRAYlON  =       200." PPM

  _I?M.p.f?*iyM. '= 200.0 DEC. _F	
              S02""CO'NC"ENtR"ATION.        ACIOTOADTNG	"
      STAGE         PPM             LBS ACID/LB CARBON
  ..__._._	•i'y.ii::y•:!.:,,, .  :;V;V; 2000.            l:^":1-  ' 0• !837__ . ••..
         2            1586.                   .671413
         3            1136.                   0.0952
         4             680.                   0.0486
                       '.275. •:£:y%j^£^%;:&.,.,.;.c
 -TQJ.A.i .PA_R._60N REQUIRED -	46.94 INCHES	n	
: TYOTAL "STAGEST REQUIRED... ASSUMING^ aOJ^CHES^

L^SPACE.  VELOCI TV.. « 	2744<'ffiHRj^

  PRESSURE  DRCP ACROSS CARBON =    23.47  INCHES  H20
  PRESSURE  DROP ACROSS PLATES_=	  I K73_ INCHES  H20 . _   „„_
f TOTAL  PRESSUR'E"DROP"rAC"RdSS" STAGes"=.;i.  35,20  INCHES  ;H20 :  :v
                             193

-------
      S02 SORBER DESIGN
 HUN NUMBER
         TEST-20   DATE   7  27  71
 TOTAL  CARBON RATE = 50.64_0_LHS/HR	
"OUT L C T C A R B ON U6 A f) ING" = " O . l"8 3 7 5" L B S A CI 0 / L 8 C A~RB 0 N"
 HiflGHT OF CARBON/STAGE =   9.00  INCHES    :. .
 DIAMETER OF VESSEL = 1_8.0  INCHES, .,...;.-. ^.•..••^4\---t''\
 CARBON USL:l)"=  	  0.""	
 TIITAL  GAS f:LOW RATE =    18969.  SCFH
 INLET  SC2 CONCTNTRATION =	2000. PPM
 'INLLT  NO CGNCENTRAI IUN = "    Tf->6.~
 INLET  02 VOLUME FRACTION =  0.0460
 INLET  H20 VCLUME FRACT I CN_=_ 0.1 f>00
 OUTLET S02" CO.NCENTRAT ION -"
                               "PPM
                             200. "PPM
 TEMPERATURF. =200.0 DEG._F _
          "~Sb2""CONClENTRAT'lON'"
     STAGE         PPM
   2
   3
    _
0.21
                    _
                    1452.
                     856.
                   __ 302_.
                 200.0001;
   ACID LOADING
L8S ACIO/L8 CARBON
         0.1837 _
        "071277"
         0.0665
         O._0098
        "0.0  "
 TOTAL CARBON REQUIRED =      37.93  INCHES
 TOTAL STAGES REQUIRED ASSUMING  9.00  INCHES CARBON/STAGE
                                                      =  4.21
 SPACE VELOCITY =
                  3396.  l/HR
 PRESSURE DROP ACROSS CARBON =     18.97
 PRESSURE DROP ACROSS PLATES =      9.48
 TOTAL PRESSURE DROP ACROSS STAGES  =
                                    INCHES H20
                                    INCHES H20
                                    28.45 INCHES
                    H20
                           194

-------
      S02  SCRBER DESIGN

RUN  NUMBER   TEST-21    DATE   7 27 71

TOTAL CARBON RATE = 50.640 LBS/HR
OUTLE T""CARBON LOADING "*""b7llT375TBS""A'CTD7rB'~'C'AR'BON"
HEIGHT OF CARBON/STAGE  =   9.00 INCHES'":      :.    ,
DIAMETER  OF VESSEL = 18_.J)_ INCJHEJJV^ _ '^^^ ^  . ;:-':
CARBON USED" =~Cf.~"    "	          '~~^~      ~
TOTAL GAS FLOW R-ATE-=     18969. SCFH
INLET S02 CCNCENTRATION_=__ ,___ 2000. PPM
J'NLE T :NQ':TONC t-NTR AT i ONT =~V~  - A so".;
INLtT 02  VOLUME FRACTION*^ :'!ol0460'   :":-".
INLET H20 VCLUMb FRACTION =  ,0.20pp_   _
CUTLET SW CONCENTRATION "=   '   "200V PPM

V . | i
STAGED
2
3
0,66
i.E ='20Q;o DEC. F
j |/I T ',*'•' ~
' : •"' PPM
1335.
618.
200.0001
•i .. •'.: '"• rMu! I!.-.
ACID LOADING T
v LBS ACID/LB CARBON ; : r;:.
0. 1837 ' C •:
. 0.1156
0.0422
0.0
"TOTAL "CARBON REQUIRED =      32.90 INCHES
TOTAL  STAGES REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE  = 3.66
 SPACE  VELOCITY = "  ;.   39T5^"l/HR

JPRESSURE CROP ACROSS  CARBON  =;  16.45 INCHES H20	
 PRESSURE DROP 'ACROSS "PLATES' =     8.23 INCHES H20
 TOTAL  PRESSURE DROP ACROSS  STAGES =    *24.68  INCHES  H20
                         195

-------
                 APPENDIX A-9-5

EFFECT OF THE INLET S0£ CONCENTRATION ON THE TOTAL
     CARBON BED DEPTH REQUIRED FOR 90% REMOVAL
                          197

-------
       S02 SORBER DESIGN

 RUN  NUMBER   TEST-35   DATE  7 27 71

__TOTAL  CARBON RATE = 12.690 LBS/HR
 OUTLET CARBO~N LOADING = 0.10375 LBS ACID/LB  CARBON
 HEIGHT IJF CARBON/STAGE -   9.00 INCHES
 DIAMETER OF VESSEL * 18.0 INCHES     _     	...
"CARBON USED -      o.
 TOTAL  GAS FLOW RATE =    18969. SCFH
 INLET  S02 CONCENTRATION =      500. PPM
 INLbT  NO CONCENTRATION =  "  150. PPM   "	"
 INLET  02 VOLUME FRACTION *  0.0460
 INLET  1120 VOLUME: FRACTION =  .0.1300	
'OUTLET S02 CONCENTRATION =       bo. PPM

_TEMPERATURE = .200.0. DEC.. F
STAGE
1
2
0.69
S.02 CONCENTRATION
PPM
500.
237-
50.0000
ACIO LOADING
LBS ACID/LB CARBON
_ . 0.1837 .
0.0761
0.0
  TOTA1,  CAHPON RF.QUI.RED *     2.4.23 INCHES               .	
 "TOTAL  STAGES REQUIRED ASSUMING 9.00  INCHES CARBON/STAGE  = 2.69
_S.PACE ..VELOCJ.IV._=	5.3_16_._L/HR	
 PRESSURE  DROP ACROSS CARBON =    12.12  INCHES H20
_PReSSUR.E_URtJP_.ACR.Q.SS.P_LAT_ES._5	&._06_JJ-JC_H.E5_H2_q
 TOTAL  PRESSURE DROP ACROSS STAGES =     18.17  INCHES  H20
    RATE  EXPRESSION USED IN DESIGN CALCULATIONS
 RATECIII=COEFF  *  (1-X(I)/XS)**A * (YS02**BI *  (V02**C)  * (YH20**D)
    WHERE  COEFF-K  *  EXPI-E/R*(II iT*460)))
          T=     200.         XS=    0.38       Y02=    0.046      YH20*   0.130
      -E/R"    5520.          A=   1.000         B=    0.400         C=   0.630          U=    0.730
        _.K"0.000159	_..._._  ..	__	_.._	.,_					_	
                                             198

-------
       S02  SCRBER DESIGN

 RUN NUMBtR   TEST-36   DATE   7  27 70

jr.U.T.AL.CARHON._RATE = 25..380 ..LRS/HR . .
 OUTLET  CARHON LOADING = 0.13375 LUS  ACIl)/l."(J"CARBON
 HEIGHT  (IF CARBON/STAGE =   9.00 INCHES
..DIAfETER  (^ .VESSEL..1. l.8.Q...HCt.CS	
 CARBON  USED -      0.
 TOTAL CAS FLOW RATE =     18069. .SCFH
_LNLE.J_S02._CP_N.C.F.MKATinN... =	looo., .PP.KL	
 INLET NO  CONCENTRATION »       150.  PPM
 INLET 02  VOLUME FRACTION  «   0.0460
 .INLET. H2C) VOLUME FRACTION =.  ..Q. U00_
 OUTLET  S02 CONCENTRATION  *       100. PPM
_JtMPLRATUKt V?00.0 DEC.  F	
             S02 CONCENTRATION         ACID LOADING
      STAGE         PPM             IBS ACID/LB CARBON
.	... .1 		  1000.			OL,.W7._	
         2            635.                   0.1092
         3            247-                   0.0299
	0.43 	LOO..OOOQ			0,.0,..__
  TOTAL  CARBON REQUIRED =      30.84 INCHES
  TOTAL  STAGES REQUIRED ASSUMING  9.00 INCHES CARBON/STAGE  *  3.43
  SPACE  VELOCITY *     4177.  l/HR      :

  ppp$«;iipp  [,qnP ACROSS CARBON ."	15.42 INCHES H20	
  PRESSURE  DROP ACROSS "LATES '      7.71 INCHES H/ll
  TOTAL  PRESSURE DROP ACROSS  STAGES =     23.13 INCHES H20
        ;. EXPJxnss.lON-USED-.JtJ.

 RATECII)«COEFF * U-XII )/XS) **A  *  =- —0.130....
          K«0.000159
                                            199

-------
       S02 SORBER DESIGN

 RUN  NUMBER   TEST-37   DATE   7  27  71

 TOTAL  CARI10N RATE = 38.060 LBS/HR
 "dilUt-T CARBON "LOADING = 0.18375 UBS  ACID/IB CARBON
 HEIGHT UF CARBON/STAGE =   9.00 INCHES
 uIAKETER OF VESSEL •'- 18.0  INCHES.  _._.. 	
 "CARBON USED =      0.
 TOTAL  GAS FLOW RATC =    18969. .SCFH
 INLET  S(!2 CONCENTRATION =	1500.  PPM     			
 "INIET'NO CONCENTRATION =       150. PPM
 INLET  02 VOLUME I'KACTION =   0.0460
 INLET  H2(l VC.LUME FRACTION f   0_.1300	  _    	
 "OUTLET so2 CONCENTRATION =       it>o.  PPM
 TEMPfcKATUKE « 200.0 DEG. F
             S02 "CONCtNlRAI ION         ACID LOAUING
      SlAGt          PPM             LBS  ACiO/LB CARBON
         1            1?>00.           _    	0. 1837
         I            1062.                   0.12'.l
         3             587.                   0.0092
         i\    	   J63._ _   	     _ _p_.00i5
      0.03         150.0001                   0.0
 TOTAL CAROON REOUIREO =     36.31  INCHES
-JfllAL S J ACE S_REQU J.KEO_ASS_UMlN.G_9_._eO  \ NCH£$_..C_ARBON./ SI AG.C__r_..'s_._03	,	

 SPACE VELOCITY =     3547. 1/HR                    .             :   '
 PRESSURE  DROP ACROSS PLATES =      9.OB  INCHES H20
J.Q.TAU._PRESSURE._DRp.P. ACROSS.3JA6Ei.«_ _2J_li4_IN£H£S..H2a	
    RATE  EXPRESSION USED IN DESIGN CALCULATIONS

..RATECU ) = COEFF * (l.-X( I )/XS.).**A * (ySD2**B)  * (V02**C) *  (YH2q**D).	
    KHCRE COEFF = K » EXPI -E/R*t I/(T + 460)))

	..  ..   T=  ..  200.  .. _    X3=    0..38	_...y02= .. 0,046.	YH20=. ,._O.J30
      -F/R=    5520.          A=   1.000          B=   0.400          C=    0.630          0=    0.730
          K-0.000159
                                                 200

-------
       S02  SORBER DESIGN

 RUN  NUMBER   TEST-38    DATE   7 27 71
_T.PTAL  CARBON. RATF =  50..75Q LOS/MR   _	   	
• OUTLET CARBON LOADING =  0.18375. LttS~AC.1 "b/LB~ CARBON"
 HEIGHT OF CARBON/STAGE  =   9.00 INCHES
_P1AMF.TF.R. OF..VESSFL *_ l8.0_LNCJiF.S	
 CARBON USED -      0.
 TOTAL  GAS FLOW RATF:  =     18969. SCFH
 IN'l.ET_SP2 CONCENTRATION  =  _  2000. PPM	
 INLET  NO CONCENTRATION  =      150. PI>M
 INLET  02 VOLUME FRACTION =  0.0160
_..)_NLET .H2Q .VG.LUME FP ACT.I ON _?.__Q, 1 300
 OUTLET S02 CONCENTRATION -      200.' PPM

_!Er,PERATURF:. '...200.0  DEC. F	
             S02 CONCENTRATION        ACIO LOADING
      STAGE         PPK             UBS ACIU/LB  CARDON
		I  		  ..2000.. ..__._.		Q.1HJ7
         2           1504.                  0.1330
         3             962.                  0.0777
		A  	     
-------
      S02 SORBER DESIGN

 RUN NUMBER   TEST-39   DATE   7  27  71

 TOTAL CARBON RATE = 63.440 LBS/HR      . .		
"CUTLET CARBON LOADING » o.13375 LBS  ACID/LB CARBON
 HEIGHT OF CARBON/STAGE «   9.00 INCHES
 DIAMETER OF VESSEL =  IB.p INCHES    		_	
"CARBON USED =      o.
 TOTAL GAS FLOW RATE =    18969.  SCFH
 INLET S02 CONCENTRATION =_  _ 2500.  PPM  	
 INLET NO CONCENTRATION =      150.  PPM
 INLET 02 VOLUMF FRACTION *  0.0460
 INLET H2H VOLUME FRACTION «   0.1300		
"CUTLET su2 CONCENTRATION =       250.  PPM

 TEMPERATURE = 200.0 DEC. F
            S02 CONCENTRATION         AC IU  LOADING
     STAGE         PPM            LBS  ACIO/LB CARBON
        1   ._      2500. .   _     .  _..... .P..J.837..
        2           1953.                   0.1391
        3           1358.                   0.0904
        4    _     _ ?62..	   	Q.041.7
        5            253.                   0.0000
     0.01        249.9999                   0.0
.TOTAL CARBON PFOUIREO «  _  45.01  INCHES
 TOTAL STAGES K( QUIRED A'SSUMING 9.00  INCHES  CARBON/STAGE = 5.01

 SPACF VELOCITY       2ft5.8.t_JL/t
 PRESSURE DROP ACROSS CARBON =    22.53  INCHES  H20
.PRESSURE DROP ACROSS PLATES.. =	 l.U27_J NCHE.S...H2.0		
 TOTAL  PRESSURE OftOP ACROSS STAGES =     33.80  INCHES H20
    RATE  EXPRESSION USED IN DESIGN CALCULATIONS
 SATECI I I^COEFF * t I.-X( 1 )/XS)**A *  (YS02**B)  *  (Y02**C)  * (YH20**D)
    WHERE COEFF = K * EXPI-E/R* ( \l ( T+'t60 I I I

         T*    200.         XS=    0.38        Y02=    0.046      YH20=   0.130   	
      -E/R*   5520.          A=   1.000          B«    0.400         C=   0.630          D=    0.730
         K=0.000159
                                            202

-------
       S02 SDRBER  DESIGN

  RUN NUMBER    TEST-40   DATE  7 27 71

_J.QtAL. CARBON. RA1E...T...76. 130 L.BS/HR ____       ___
  OUTLET CARBON  LtJAUING = 0.18375 LBS Aclu/LO  CARBON""
  HEIGHT OF CAKbON/STAGE «   9.00 INCHES
i_U.l.A^£.TfH. Qf-VE.SSE.L._«._1.8..0-IMCHES     ____
  CARBON USEO =0.              __
  TOTAL GAS FLOW RATE  =    18969.' SCFH
_lN.L,tJ_.S02_C-a/K.E.MLR-AT.LOM..r _______ JflQQ. PPM __ ____
:  INLET NO' CONCENTRATION =      150. PPM
  JNIET 02 VOLUME  FRACTION *  0.0460
L_lI4LEt_H20. VOLUME. FRACT.10N_.= __Q._l_3iiD ___ ____
  OUTLET S02 CONCENTRATION =      300. PPM

_J.EMPERATURE =_200,Q  OEG, .F ____________ . _____ _______ ._
             S02 CONCEN1RATION        ACID LOAOJNG
•      STAGE          CPM            LBS ACID/LB CARBON
_______ ..... 1 _________ .JOOO. ____________________    .O.L8J.7
         2           2409.                   0.1435
         3            1768.                   0.0998
                                              .a «
         5             316.                    O.OU5
      0.42         300.0000                    0.0
  TOTtl  r.ARRIlN RFQtltRFn =	48. 78 IMf.HF!;	
;  TOTAL STAGES REQUIRED ASSUMING 9.00  INCHtS  CARBON/STAGE = 5.42 :.-:  : ,  :

_.SAAC£ -VEI.OCI TJf_=__
  PRESSURE DROP  ACROSS  CARBON »    24.39  INCHES  W
  TOTAL PRESSURE  DROP  ACROSS STAGES =     36.59  INCHES H20
$.   •         ,-   •-,• - *'.;  .•»>..  .:  • -  •--   ••••  " ^*; -y^j^k'^
     RATE EXPRESSION  USEO IN DESIGN CALCULATIONS
  *ATECU»=COEFF *  ( l~K( I )/XS)**A * 
-------
       S02 SORBER DESIGN

  RUN NUMBER   TEST-41   DATE  7 27  71

_TOTAL CARBON.RATE =101. 500 . IBS/MR   	 . _	___..
  OUTLET CARBGN LOADING = 0.18375 LUS  ACID/LD CARBON
  HEIGHT OF CARBON/STAGE =   9.00 INCHES
_DIAMF.THR OH VESSEL = 18.0.  INCHES.		
  CARBON USED *      6.
  TOTAL GAS FLOW RATC =    10969. SCFH
_ INLET S02 CONCENTRATION «_    _4QOC).  PPM  __
  INLCT NO CONCENTRATION =       150. PPM
  INLET 02 VOLUME FRACTION =  0.0'<60
  INLET H20 VOLUME FRACTION ?_  .0.1300			
  OUTLET SU2 CONCENTRATION =      400.  PPM

 _TEMPFRATURE = 200.0 DEC-. F   _     .      ._.	  .
             S02 CONCENTRATION         ACID LOADING
      STAGE         PPM            IBS  ACID/LB CARDON
_       1           4000.        _  		0.. 1837    ..
         2           3332.                  0.1496
         3           2612.                  0.1128
 _       4	      1867.	   0.0747
         5           1143.                  0.0377
         6            510.                  0.0054
	.0...2Q	4QQ nO.QO.0.	J3,0		
  TOTAL  CARBON REQUIRED =     55.79  INCHES
  TOTAL  STAGES REQUIRED ASSUMING 9.00  INCHES  CARBON/STAGE  = 6.20
  SPACE  VELOCITY =     230<3, 1/HR

_RRESSURE .DROP. ACROSS..CA.RBON •-:	?.7.9D_IilCHESi_H2D	
  PRESSURE DROP ACROSS PLATES '-    !.3.95  INCHES  H20
  TOTAL  PRESSURE DROP ACROSS STAGES *     41.84  INCHES  H20
    ..RATE.JXPRCSS10N USEQ..JN -DESIGN CALC.ULAT.IONS.
 RATECII)=COEFF * (1-XII)/XS)**A *  (YS02**B)  *  (Y02**CI  * 
-------
                  APPENDIX A-9-6

EFFECT OF THE INLET SC>2 CONCENTRATION ON THE TOTAL
      CARBON BED DEPTH REQUIRED TO ACHIEVE AN
        OUTLET S02 CONCENTRATION OF  100 PPM
                           205

-------
       $02 SCROER DESIGN

  RUN NUMBtR   TEST-36    DATE  7 27 70

_TDL4J._£ AR BON...R 4 T E. ..= .2_5_.J 8 0_Lfl SZHR_
  OUTLET CARBON LOADING  «  0.18375 LBS ACID/LB CARBON
  HEIGHT (IF CARBON/STAGE =   9.00 INCHES
  CARBON USED =       0.
  TOTAL GAS FLOW  RATE  =     18969. .SCFH
  INLET SQ2 CONCENTRATION,*	1.00
-------
      S02  SURBER  DESIGN

 RUN NUMBER    TEST-49   DATE  7 27 71

JLOT.AL CARBON. .RATF  =03.570 LBS/HR
 CUTLET CARBON  LOADING = 0.18375 LBSACID/LB CARBON
 HEIGHT OF CARBON/STAGE =   9.00 INCHES
 OJAHETER  OF  VESSEL _= 18.0 INCHES_	
"CARBON USED  ^       o.
 TOTAL GAS FLOW RATE =    18969. SCFH
_INLET SQii CONCENTRATION .5   _ 2000.  PPM  	
 "INLET NO  CONCENTRATION '=     "I"*O"."PPM"" "   "	"~
 INLET 02  VOLUME  FRACTION -  0.0460
 INLET H20 VOLUME FRACTION *  0.1300  _	
 OUTLET S02 CONCENTRATION -      lOO.Vf'M

 TtMCtRATURL  =  200.0 OEG. F
            S02 CONCENTRATION        ACIOLOAOIHC"
     STAGE          PPM            LBS ACIU/L8 CARBON
        1            2000,               _ Q.l(!37
        2            liO-V,                  6.13^7
        3             968.                  0.0838
        A             451.     	   _     Q.Q338
	"O.B«       "166.0060                  6.6
 TOTAL CARBON  RFQUIRFO =     43.90 INCHES
__TQTAL_S.TAGES. REQU IReO_ ASS.UM I NG. 5, .OJJ..I NCHE.5._ CARBON/ STAGE _=__4.88__

 SPACE VELOCITY =      2934. I/HP.
 PRESSURfc  UKUP  ACROSS CARbOH =    21.95 INCHES H20
 PRESSURE  DROP  ACROSS PLATES =    10.98 INCHES H20
 _TOTAL_PRESSURE DROP ACROSS STAGES_=	J2.93_INCJ1ES_H20__
    RATE  EXPRESSION USED IN OESIGN CALCULATIONS

        l )=COEFF  *  (1-XI1 1/XSI**A *_ ( YS_C2**B I. * _ I Y02**C ) *._LYH2a**PJ.	  			
    hHERE  COEFF=K  * EXPt-E/R*(I/(T+460)))

          T=    200.        XS=     0.38       Y02=	0.0'.6_	._ YK2P5...  0.110    	 _	 	
      -E/R=    5520.         A=    1.000         B=   0.400          C»    0.630          0=   0.730
          K=0.000159
                                             207

-------
       S02 SORBER  DESIGN

  RUN NUMBER    TEST-50   DATE  7 27 71

_TOTAL CARBON.RAU  = 11Q..OOO LRS/HR	
  OUTLET C AC, II ON  LOADING = 0.18375 LHS ACIU/LB CARBON
  HEIGHT Or CAROON/STAGE -'  9.00 INCHES
  OlAMEH* uf VESSFl,_=L IB.Q INCHSi. ____________ __
  CARIHJU USED -       0.
  TOTAL GAS FLOW RATF =    18969. SCFH
  INLI 1 SO? COUCrNTP.AT10N_=.     .4000. ..P.PM ____________________
  INLET NO CONCfcNfUATlhN "=      150. PPh
  INLET 02 VOLUME  FKACT10N =  0.0460
  INLET ll^O VO.LUMb FRACT[ON. = ___O.UOO.__. ____________ . _______
  OUILEI S02 CONCENTRATION -      100.  PPM

      E MATURE =.200.0 DfG. f  ..... ____ .._  ....... _ ....... .
             SC12 CONCENTRATION        ACID  LOADING
      STAGt          PPM            LBS  ACIU/Lli CAkOON
         1    ...   .   .3000., ....... __________ ...... 0..1837 ......
         2            3332.                   0.1523
         3            2620.                   0.1187
        ..'t         ..  186"?, ______ ___ ...... _______ 0.08
-------
                 APPENDIX A-9-7

EFFECT OF THE INLET SC>2 CONCENTRATION ON THE TOTAL
  CARBON BED DEPTH REQUIRED TO ACHIEVE AN OUTLET
            S02 CONCENTRATION OF 50 PPM
                           209

-------
       S02 SORBER DESIGN

  RUN  NUMBER   TEST-35   DATE  7 27 71

 _LPTAL CARBON RATE  = 12.69Q.L6S/HR
__                          .
r  OUTLET  CARBOli LOAUING = 0.18375 LBS ACIO/LB CARBON      .'
i  HEIGHT  UF  CARBON/STAGE »   9.00 INCHES             .    i  . •- '.
LPJAMETER  OF_V£SSEL_=_ la.q INCHES ___     •••' • ":. .-.. -'"}.
 CARBON USED «       0.
 TOTAL  GAS  FLOW RATE =     18969. SCFH
_1NLET  S02  CONCENTRATION =	500. PPM	
f: iwit'i  NO CONCENTR'ATION' =~    "isb. PPM
I. INLET  02 VOLUME FRACTION «   o.04&o
L.INIE.T  H20  VOLUME FRACTION =	Q._130.Q	
 OUTLET SO? CONCENTRATION «        i6.  PPM

 TEMPERATURE -  200.0 DEC. f
£.'v •'••:. STAGE
1
2
0.69
S02 CONCENTRATION
PPM
500.
237.
50.0000
ACID LOADING ;i ; .;: -
•>'LBS ACID/LB CARBON, ••••'•';. '••. "•'' , i-;™' -' •. -'?•... : s •. ••;. ••• , .•• •'••'.?.'" •• •: >
0.1837 :.. ! ."..
0.0761
0.0
        CARBON_RE9UI.REO  =   __ 24. 23_ INCHES.
 TOTAL  STAGES  REQUIRED  ASSUMING 9.00 INCHES CARBON/STAGE = 2.69
_iPA.QE  VELOCITY  =	5316.  1/HR			

 PRESSURE  OROP ACROSS  CARBON »     12.12  INCHES H20
/PRESSURE  DROP ACROSS  PLATES =      6.06  INCHES H20	„	
 IUIAL  KKtSiUkt  DROP ACROSS  STAGES =     18.17 INCHES H20
I-: :: RATE EXPRESSION USED  IN  DESIGN  CALCULATIONS
 RATECU ) = COEFF *  Il-X (I I/XS)**A  *  (YS02**B)  * (Y02**C)  * (YH20**D)
    WHERE COEFF-K  » EXP(-E/R*(I/IT+460)))
         T«    200.         XS*     0.38        Y02«    0.046      YH20«=   0.130
      -E/R*   5520.         A»    1.000          B-    0.400         C«   0.630          0»    0.730
   	_.K-0.000159.	,	,	'.	L.	.	
                                              210

-------
     S02  SI1KBER DESIGN

RUN NUHHFR    TFST-'jl   OATP   7 27 71

TOTAL CARBON RATf = 5" 1 Ysu2**o"r *  (Y02*'*cT~*"TYH2ov*br
    WHtRH CUEFF'K *  EXP(-E/«*I 1/(T+'.601 I I
         I>    200.
      -E/R«   5520.
         K'O.000109
                                  '67Ja"
                                  i.ooo
Y02"
  B=
0.046
0.400
"YH26-
    C-
0.130
0.630
0.730
                                             211

-------
        S02  SORBER DESIGN

  RUN  NUMBER   TEST-04    DATE   7 27 71

_J£TAL  CARBON RATC *lll«.4PO LBSVHR	
  OUTLET  CARRON LOADING =  0.18375 IBS ACID/IB CARBON
  HtlGMT  OF C.ARBCJN/STAGC  =   9.00 INCHES
_PIAMCUK  OF. VfSSEL...!L.18.«.D_LMCJi£i__	
  CARBCN  USfcU =      0.
  TOTAL  GAS FLOW RATE =     18969. SCFH
	1 .NLE 1_ .S.O.Z. ..C.ON.C.E NT P. AT_.LO.N_=	A 0_00._ P P.M	
  INLET  HU  CONCENTRATION  =       150. PPM
  INLET  O/  VClUf-r FRACTION  *   0.0460
             VOLUME F.RAC.T1QN_* ._0,JJQP_
  CUTLET  SU2 CONCENTRATION  =        50. PPM

  JEMPCRATUKt = 200.0 DEC.  F     _..  	
              S02 CONCENTRATION         AC I 0 LOAOJNG
      STAGE          PPM             IBS AC10/LB CARBON
 .	   1     . .__    4000.          _	Q.1837_
          2            3332.                   0.1527
          3            2621.                   0.1195
 _......   Jt ...  ...-'-.	 1893,	,		..0.0656... ...
          5            HUB.                   0.0528
          6      '       567.                   0.0239
 		_I	115.	Q.QD.Sfl	
      0.25.         -50.0000                   0.0
  TOTAL CARBON  RFQUIP.ED =     65.21  INCHES
._TOTA( MAUI-S  RbUUIRfcO AS!>UnlNL.      5520.         A«    1.000         B«    O.'iOO         C=    0.630         0=    0.730
          K=0. 000159
                                              212

-------
                 APPENDIX A-9-8

EFFECT OF THE OUTLET H2S04 LOADING ON CARBON ON THE
   TOTAL CARBON BED DEPTH REQUIRED TO REMOVE 90% '
     OF AN INLET S02 CONCENTRATION OF 2000 PPM
                     213

-------
       S02 SORBER DESIGN

  RUN NUMBER    TEST-7    DATE   7  27  71

  TOTAL CARBON  RATE  = 50.640 LBS/HR
["OUTLET CARBON" LOADING  =  0.1837.5  LUS  AC ID/LB~CARBON
i  HEIGHT OF CARBON/STAGE =
I  DIAMETER OF VESSEL  =
  _
  CARBON USED =      0.
  TOTAL GAS FLOW RATE =     18969.  SCFH
  JNLET S02 CGNCfrNTRATlQN_j=	2000^ PPH
  TNYETWO~TONCENTRATlON  =    :,,  150~7 .
  INLET 02 VOLUME FRACTION  =  '0.0460
  INLET  '20VCLUME  FRACT I CN ~  0.
  OUTLET S02 CONCENTRATION  =       200.  PPM

  TEMPERATURE = 200.0 DEC.  F
< - STAGE
^ 1
2
3
S02 CONCENTRATION
PPM
2000.
1504.
962.
438.
,ACID LOADING ,,;%•: -:,.^^f, + .- . .
LBS AC 1 D/LB C ARBON ^f^fe^;' .'•.;
0.1837 ,^:s::yUSil? ^A?- ; /
0.1329
0.0774
0.0237
  TOTAL CARBON REQUIRED =     40.76  INCHES
  TOTAL STAGES REQUIRED ASSUMING  9.00  INCHES CARBON/STAGE = 4.53
|: SPACE VELCCITY.,=;;;;;4:g3i:61r;^
                                                         :I:S?^^*^as;'
  PRESSURE DROP ACROSS  CARBON  -     20.38 INCHES H20
  PRESSURE ORRP ACROSS  PLATES  =     10.19 INCHES H20
  TOTAL PRESSURE DROP ACRCSS STAGES =     30.57 INCHES H20
                            214

-------
       S02 SORBER  DESIGN

  RUN NUMBER    TEST-16   DATE  7 27 71

  TOTAL CARBON  RATE  = .50_^40_ L__BS/HR	
  "OUTLET cARBONToADiNG = o.oTrel LBS ACro7lT~cAR'BON"
  HEIGHT OF CARBON/STAGE =   9.00 INCHES
  DIAMETER OF VESSEL = 18j.O__I_NCHES	„____	
  "CARBON usED"-^	cT. "       ^ '•' '       ""
  TOTAL GAS FLOW  RATF =    18969. SCFH
  INLET S02 CONCENTRATION =_	2000._PPM	
  INLET NO CONCENTRATION"^""  """ ~II>O.~P"£H~~:':.  ~
  INLET 02 VOLUME  FRACTION =  0.0460    ::   : :
  INLET H20 VLLUME FRAC.] I CN_f___p_._l_300 ___	
  OUTLET" so2 coNCENTRAnoN =      200". PPM"

  TEMPERATyRE = 2.00.0 DEG_._F	    	
           "r'sdY""CONCENTRATION     "  ACID LOA'D'ING
   :   STAGE:;     .    PPM          .  LBS ,ACl D/LB CARBON
                      2000.                  0.0919
         2            1291.                  0.0192
         3             588.                  0.0
      0.75         200.0001                  0.0
  TOTAL CARBON  REQUIRED =     33.76 INCHES
  TOTAL STAGES  REQUIRED ASSUMING 9.00 INCHES CARBON/STAGE  - 3.75

r"TpATEnin!UbciTY^                               ••,:, -rii^^^C^

?  PRESSURE  DRpP_ACRgSS CARBON V\:   16;88  INCHES  H20 ::'.'' ^Lj^LJ-••;.•::•?'••
""'PRESSUR'E "DROP ACROSS'TLAT'ES =    " a"."^4  INCHES""H2"o"
  TOTAL PRESSURE DROP ACROSS STAGES =     25.32  INCHES  H20
                             215

-------
      S02 SORBER DESIGN
 RUN NUMBER
TEST-17   DATE  7 27 71
 TOTAL CARBON RATE = 50-640  LBS/HR     	
 OUTLET "CARBON LOADTNG"'= 0". 27"562 WS "AC I DTOTTlARBON
 HtlGHT OF CARBON/STAGE =    9.00  INCHES   " i:. • ;:v.. v. :J  :;
_DUMETF:R OF VESSEJ. = _18.0 INCHES	^JlIilMliS^-'^
 CARBON "USfcD"="""  ~ 0.
 TOTAL GAS FLOW RATE =     18969.  SCFH
 INLET S02 CONCENTRATION =   _   2000. PPM_    __
 INLET NO CONCENTRATION'--    "  TSO.'PPNT"   ;'•--—-
 INI.ET 02 VOLUME FRACTION  ~  O.OA60        A',. ••
 INLET H20 VCLUME  FRACTICN =__0^1300    _^_  ;  _
 OUTlET SU2"CCNCCN'TKATfUN""-"""    "200. "P'PM
 TEMPERATURE = 200.0 DEC. F
            "502 CONCENTRATION
     STAGE
        __
        5
     0.32
    :PPM
    ,.  2000
  "ACID LOADING
LBS ACID/LB CARBON
         0.2/56  :...;'
                    1409.
         _
       665.
         0.2't79
         0.2151
         0.1780
           1388
           1019
   200.0001
0.
0.
0.0912
 TOTAL CARBON REQUIRED =    ;  56.90  INCHES
 TOTAL STAGES REQUIRED ASSUMING 9.00  INCHES CARBON/STAGE-^ 6.32
 SPACE  VELOCITY =
        2264. 1/HR
 PRESSURE DROP ACROSS_CARBCN =  	_28_.45 J_NCHES H20    __
"PRESSURE DROP" ACROSS "PLATES'^    "14.22  INCHES "H2o"
 TOTAL  PRESSURE  DROP ACROSS STAGES =     42.67 INCHES H20
                           216

-------
      S02 SOR8ER DESIGN

 RUN NUMBER   TEST-18   DATE   7 27  71

JJ?TAk CARBO_N RATE = 50.640 LBS/HR
 CUUETCA~RBCN 'LOADTNG" = 0%3675~0  LBS~ ACTD/TF
 HEIGHT OF CARBON/STAGE =   9.00  INCHES
 DIAMETER QF yESSEL = 18.0 INCHES
"CARBON'USED~ = '"
                         CARBON
0.
 TOTAL
 INLET
"INLET
 INLET
 INLET
 OUTLET
                PPM
GAS FLOW RATE =     18969.  SCFH
S02 CONCENTRATIONI _=	_200p.  PPM
NO CONCENTRATION"^   "   "156".
02 VOLUME FRACTION  =  0.0460
H 20 VOLUME F R ACT! ON  -   0_._l 3 0 0_
 S02" CONCENTRATION  =   " 	"
             200. PPM
 TEMPERATURE = 200.0 OEG._F  _
           "S"02 CONCENTR AT ION
     STAGE         PPM
        l.:'.-:'-.-:'"V- . -    2000. •'•••••••T
                 ACTt5 LOAOTNG" "
              LBS ACID/LB CARBON
              ;         0.3675
2
3
4
5
6
/
8
9
10
n
12
13
14
0.38
1967.
1925.
1872.
1806. .,«
'1723. "3 \
1 622.+. T^
1498.
1348.
1173.
970.. -vx
7 4 6. ••'•;;•£
510. :?
281.
200.0001
0.3641
0.3598
0.3544
^.::f:.:*.:-..?,i*;.:^.:-.<.. 0.3476 , .: ••:•-/•: •;..
;:::;>i:•M:ii::;i..tr^,:::.::iC:v•:r:,v.:i•.••o ^^qi ' ..••;:> ;-:- ;--r. ":
-.;•. .v.;.::::v:*'f •.?:..'. T;V,:, -Af-:.:, .', U * * * J L : - '. - .•-..••,
••^•••^•^^'^•^}:-'- 0.3281 :••'.••• '..:• . ;•=•••:••:••
0.3160
0.3008
0.2827
'^:::,K^-m'(<:m^----: ' ;.; 0.2620
^i^liJiitiiSW'f :i';-:-' 0. 2390
::;::t^!Nv|!|5-:;;i:;:^?::::l:', 0.2143
0.1914
0.1831
JOTAL CARBON R F_Q UIR iD _=_ _ ili*:38  I NCHESl	.	,	
 TOT'AL"S"TAGES"REQUTRED~ASSUMING  9.00  INCHES CARBON/STAGC =14.38
 SPACE VELOCITY =
   996. 1/HR
 PRESSURE DROP ACROSS CARBON =     64.69  INCHES H20
_PRESSURE DRCP ACROSS P_LATES _=_ _32 ._34_JNCHES H20	
 TOTAL PRESSURE DROP ACROST STAGES =     97.03 INCHES H20
                           217

-------
                   APPENDIX A-9-9

EFFECT OF THE TEMPERATURE ON THE TOTAL CARBON BED DEPTH
 REQUIRED TO REMOVE 90% OF AN INLET S02 CONCENTRATION
                      OF 2000 PPM
                       218

-------
      S02 SORBER DESIGN

 RUN NUMBER    TEST-7   DATE  7 27 71
 TOTAL CARBON RATE =_
"OUTL'ET" C "ARBOirLOAD ING
 HEIGHT OF CARBON/STAGE =
_DIAH E1ER_OF_VESSEL = 18.0
 CARBON "US ED" =
 TOTAL GAS
       S02
      "NO""
                     50JL640J.BS/HR
                       = . 0."1837.5
                          LBS  ACt.D/LB  CARBON"
                     :9.00 INCHES.
                     INCHES
JNLET
 INLET
 INLET
 INLET
 "OUTLET
             o.
    FLOW RATE =     18969.  SCFH
    CGNCENTRATION_f_	2000. PPM
   CONCENTRATTON =    .:,, 150.  PPM"
02 'VOLUME
                 FRACTION =
                  P R ACT I CN =
   150
: 0.0460 v
 :;,0 . 1 300
 S02 CONCENTRAlON =
                                 200.  PP'M
            _= 200 <._^ 	
            S02"CONCENfRAflON
, STAGE
; i
2
3
PPM
2000.
1504.
962.
438.
LBS ACIP/LB CARBON
0. 1329
0.0774
0.0237
                ^2 00,000 i::,
                                            0.0
 TOTAL CARBON REQUIRED =     40.76 .INCHES
 TOTAL STAGES REQUIRED ASSUMING 9,00  INCHES  CARBON/STAGE = 4,
                                                              53
 SPACE VELOCITY =
                      3161. 1/HR
 PRESSURE DROP ACROSS CARBON =    20.38  INCHES  H20
 PRESSURE DROP ACROSS PLATES -    10.19  INCHES  H20
 TOTAL PRESSURE DROP ACRCSS STAGES =     30.57  INCHES H20
                           219

-------
      S02 SORDER DESIGN

 RUN NUMBER   TEST-22   DATE   7  27  71

 TOTAL CARBON RATE = 48.790 LBS/HR
 OUTLET CARBCN LOADING = 0.18375  LBS  ACID/LB CARBON
 HEIGHT OF CARBON/STAGE =   9.00  INCHES
_OIAMETCR OF VESSEL = 18.0.. INCHES  .;•   -v -:::;;;.'•'::;• <-v::  ^__
 CARBON USEO~=0.	
 TOTAL GAS FLOW RATE =     18276.  SCFH
 INLET S02 CCNCENTRATIO_N_= _ __200_0_._  PPM	
 INLET NO CONCENTRATION "-" "	TSO". PPM~ " ."."
 INLET 02 VOLUME FRACTION  =  0.0460    .<  .  ;
 INLFT H20_ VOLUME FRACTION  -  0. 1300  '''''"'.
 OUTLET s"02 "CCNCENTRATION"^"      2601 "PPM"

STAGE
1
2
3
4
5
0.52
S02 CONCENTRATION
.PPM • - "•.. : ,:••;.•
. ..'.:;, . 2000. i. i .
1615.
1198.
771.
376.
200 . GOO 1
ACID LOADING
•-•. LBS ACID/LB CARBON A :*
.:;i:;::.:-'-;".;:'::-'.. :•:•••• 0.1837 /:\,":^^:
0.1443
0.1016
0.0579
0.0174
/•* rs
w * o
       CARBON_   _		
"TOTAL"STAGE'S "REQUIRED. ASSUMING  9".oo""iNcvrE"sT'CARBON/sTAGF;=  5T52

SPACE  VELOCITY =     2498.:1/HR:
 PRESSURE  DROP ACROSS CARBON =     24.84 INCHES H20
 PRESSURE  DROP ACROSS PLATES =_  _L2'42 INCHES H20
 TOTAL  PRESSURE DROP ACROSS" STAGES ="'T 37.27" INCHES ~H2lf
                               220

-------
      S02  SCRBER DESIGN

RUN  NUMBER   TEST-23    DATE   7 27 71

TOTAL CARBON RATE = 47.070 LBS/HR
OUTLET "CARBON LOAD I N(T ="'OVl 8375~niT"^CTiJ7rB~C"7rRBON'
HEIGHT OF CARBON/STAGF.  =    9.00 INCHES
DIAMETER  OF VESSEL =_l_8_.0  INCHES ::
CARBON USED =	0.   '"       ~  ———     ~
TOTAL GAS FLOW RATE =     17633. SCFH
INLI-T SG2 _CCNCENTRATION =_    2000_. PPM
"INLF. T NG~'CONCENTRAT ION "="       T50- ~"PPM""""~™~"™:~"
INLET 02  VOLUME FRACTION  =  0.0460   '.:-.--.''x '•'• • • ::'^^\ • •
INLET H20 VOLUME '-RACTICN_^	9_«J._300     :;;..: . :..':^:.:.;•-
"OUTLET S02" CONCENTRATION"^      200T"PPM  —-^   :-
TEMPERATURE
| STAGE.....
2
3
. 6
0.71
= 250.0 DEG. F
S02 CONCENTRATION
, ;.; : PPM
:''::•'•.: I'T.^:--" 2000'.'
1697.
1371.
1033.
2CoJoQr-fiiiSl


ACID LOADING
LBS ACID/LB CARBON
0. 1837
0.1527
0.1193
0.0846
:;,::;,-::s,;;::--.:-,:: ,,.,..: 0.0503.
?f:p^d^::;--. .-o.oias:
Wfiti&t&ti'-L 0..0

YOTAL":CARBON""REC!U"IRED  =   ;  ;60".37
TOTAL  STAGES REQUIRED  ASSUMING 9.00 INCHES  CARBON/STAGE = 6.71
SPACE  VELOCITY =      1984.  1/HR

PRESSURE DROP ACROSS  CARBON _=	^P.-1?  INCHES  H20
PRE SSURE DRCP' "ACROSS"~PL ATES" -' ""  "f5 .09""lNCHES""H2'd	""
TOTAL  PRESSURE- DROP ACROSS  STAGES =     45.27  INCHES H20
                               221

-------
     S02 SORBER DESIGN
 RUN NUMBER
             TEST-24    DATE  7 27 71
 TCTAL CARBON RATE = 45.470  LBS/HR  _
"OUTLET CARBON LOADI "NG~~ =  O.T8375 TBS ATTD7LO~T7iRBON'
 HEIGHT OF CARBON/STAGE =    9.00  INCHES
 DIAMETER OF VESSEL_= i?_._0__INCHES__	|	
"CARBON USED~=~~    o.
 TOTAL GAS FLOW RATE =     17033.  SCFH
 INLET S02 CONCENTRATION  ^_ __  200°'_ ?P1
 INLET NO CONCENTRATION -  "   "	i'50T "PP"M~
 INLET 02 VOLUME FRACTION  =   0.0460     :
 INLET H20 VOLUME FRACTICN_=   0.1300  -:
"OUTLET""S02"CCNCENTRAT ION  =
                                    __
                                 ^OO.'P'PM"
TEMPERATURE =  275.0  DGG.  F
            S02
STAGE :
                   PPM
                                     "AC rO"'LO'AD"lNG' .......
                                  L8S ACIO/LB CARBON
1 •.. -:-
3
4
*>

6
: 7
8
0.10
',. 2000.
1758.
1500.
1231.
957, :

688 . ;. j:>
220.
200.0001
'.• •"• V s : o.i837
0.1589
0.1325
0. 1049
₯,:v.-:-../.-: .-.-vxaV; .;,-:'..•:-., 0.0769

;.:gi:x:|-: x;:.; ^-:^.ff:yr, ?:?T: ; : : . Q . 0 4 9 4
f E^Miilll^ll^lC: 0.0236
0.0014
0.0
 TOTAL CARBON REOU IRED_ =___   7 2_._9 4 ^I_NCH E S  ____     ___ _
"TOTAL STAGES REQUIREl)~ASSUMfNG 9.00 INCHES CAR~BW/ STAGE
                                                          ____
                                                          = 8.10"
 SPACE VELOCITY =
                      1586.  1/HR
 PRESSURE DROP ACROSS  CARBON  =;;
 PRESSURE DROP ^CRO'SS|]-AT_§S__=_
                    "
                                  36.47:  INCHES  H20
                                  18.23  INCHES  H20
 TOTAL PRESSURE DROP  ACROSS  STAGES =
                                         54.70  INCHES H2O
                          222

-------
      S02 SORBDR  DESIGN

 RUN NUMBER    TEST-25   DATE   7  27 71

 TOTAL CARBON  RATE = *1.*980_ LBS/HR
 OUTLET CARBON  LOADTNG~= "O'Tl"8375~H'S"~AC1 WLTfTTRBOW
 HhlGHT CF CARBON/STAGE =   9.00 INCHES
 DIAMETER OF V E S S EJL_ =_ 18 . 0 _INCHIES_^         	
"CARHON"USEDi •="•"   ~ o."~	*  '       ~"
 TCTAL GAS FLOW RATE =     16473. SCFH
 INLET S02 CONCENTRATION =    _j?000_.  PPM _
 INLFT NO "CONCbNTRAT ION""= '"	" " l50V "PPM':'~
 INLET 02 VOLUME  FRACTION =  0.0460    .;•'"•
 INLET 1120 VOLUME FRACTION =__0_.J3qO  _ ::;^
 OUlLliT S02 CONC'ENTRAtTON""^" " '   "2'66. ~P"P~M"

 TtMPERATURE =  300.0 DEG. F
'	  •	~s"o
     STAGE  . .
        2
        3
        8
        9
     0.72
;ONCENTRAf I'ON~" ""
PPM
•:• •;.; .2000.
1803.
1596.
1380.
115«,
0-3 C
^ ^ ^ *
716.
508.
319.
200.0C01
ACID LOAD ING" 	 ~" ~"
L8S ACJO/L8 CARBON :
' .0.1837 ./%••: :.'.
0.1636
0.1423
0.1202
0.0975 	
0 07^7
0.0522
0.0309
0.0115
0.0
 TOTAL 'CARBON'Rif"QUTREU~=      87.44 INCHES"
 TOTAL STAGES  REQUIRED ASSUMING  9.00 INCHES CARBON/STAGE = 9.72
 SPACE VELOCITY  =.;,;,. ' 1279.  1/HR; \;-,,:..:f.'-M;,.,::;,:V: : ;.,.^?i> •:,:;•.>.-

 PRESSURE DROP ACROSS CARCCN  ='    43.72 INCHES  H2Q1	;___:
"PRESSURE" DROP"' ACRCSS^P'LATES' =  " 21.86 INCHES  H2b"
 TOTAL PRESSURE  DROP ACROSS  STAGES =    65.58  INCHES H20
                             223

-------
              APPENDIX    A-10
REACTION RATE STUDIES FOR SULFUR GENERATION
       IN 1 INCH DIAMETER FIXED BED
                      224

-------
                                                                 RATE OF SULFU" GENERATION
                                                                       BENCH SCALE
                                                                                                       3  10 71
CO
Ul
- SG-72

  SPACE VELOCITY
~ I'-E^T GAS  CLCV.'
 ' *F:G"T  CF
                                     O.IOO'S^E Ofc /HI
                                  T£  =       233.00 SCC/MlN
                                   UNLCAC.-FD *      11.900 G-«S
                                                                    LOADED
                                                                                   15.00 CMS
              - INLET orBCE"jT  u2s  ,      30.000
                INLET "OLAR M2S  CONCENTRATION •
                INLET SJLFURIC ACI2 LOADING •
                                       0.42B571 MOLES H2S/MOLE  INERT  GAS
                                     0.206000 GYS H2S04/GM CARBON.
                FINAL OJTL£T  PERCENT  SULFUR LOADING CN CARBON  -       is,040
                FINAL C'JTL"*  SULFUR  LOADING ON CARBOA »        0.227 CMS S/GM CARSON
              ~ INITIAL TF.-'PERAT',-°E  =      2"'C.CO F
                wtxr-'jn' TEVOERATUPE  «      355.00 F
                FINAL TE^ERA-LRF  -       302.00 F
TP'E
0.0
— 2.0
4.0
7.0
- 10.0
12.0
Ifc.C
— 16.0
- 15.0
20.2
- 22.0
24.0
26.2
— 2?.C
. 3C.O
32.0
- .34.0
36.0
3S.O
— 42. C
42.0
44,0
- 46.0
4P.O
52.0
~ 57.2
; 54.2
f ~ • 0
- 5E.C
6C.O
62.0
T 64.2
6S.2-
PERCENT H2S
0.
-o.
0.
c.
- c.
0.
0.
c .
w .
0.
V •
0.
. .
' C .
0.
c.
c .
c.
2 •
— c .
•:,
C i
Oi
0,
OOOOCOE
CCOOOCE
OC'OOOOE
26CC22E
642202E
7600C2E
126002E
176000E
2C22COE
222:22E
236200E
24023CE
2-4r02E
2 5-62 CO"
264000E
272003E
2 74002E
27320CF
2 7 « 2 T 2 E
27=OC2E
'27-r-2;F
, 2 i - Z ~ C E
i272202F
i 2 5 6 2 0 T E
2.256700F
..... ^
.2602C2F
0.27222CE
.... c '
C.
2,
'j ,
c,
i27222CE
i27220CF
i2 '4CO;c
•2740C2E
.27400CE
6?.0 D.2740COF
—72.0

75iO
AC!?
C.2740-JOE

~.
LOA:
,2'4CCcE
.27402-CE
ING «
00
00
CO
21
01
01
02
22
02
02
02
02
02
02
02
02
C2
02
02
22
02
02
C2
02
C2
0?
22
">?
v £
C2
02
02
22
C2
02
02
C2
02
C.
PERCENT 502
0. OOOOOCE
0. OOOOOOE '
O.OCOOOCE
0. OOOCOOE
0. OOOOOOE
C. OOOOOOE
0. OOOOOOE
C. OOOOOOE
0.000200E
2.0002'OOE
O.OOC200E
O.OCOOOCE
0. OOOOOCE
• -• 0. OOOOOOE
0.00'JCOOE
C.CJOCOOE
0. OOOOOCE
O.COOOOCE
0.0002-OCE
	 C.COOOOCE
o.ooooocc
0. JJJO'JOE
0. OOOOOCE
0. OOOOOOE
0. OOOOOOE
— ' - O.OC002-CE
O.CC2COCE
• o. OOOOOCE
O.OJOCOOE
0.02000CE
C.COOOOOE
C.CCOOOC'E
C.OCOOCOE
0. OOOOOOE
C.OOC20CE
O.ODOOOCE
205999E-21 AT
00
oo-
00
00
00
CO
An
CO
CO
00
00
00
00
00
00
00
CO
00
00
CO
00
GO
00
00
00
00
CO
00
cc
00
00
CO
CO
00
00
00
00
c.
PERCENT coz MOLAR CONC HZS
0.
	 o.
0.
c.
0.
c.
0.
0.
0.
0.
'" ~ 0.
0.
f.
c.
OOOOOOE
OOOOCOE-
OOOOOOE
OOOOOOE
OOOOCOE
OOOCOOE
OOOOUCE
OOOOOOE
OOOOCOE
OCOOC-OE
OOCOCCE
COC2.VOE
OOOOOOE
OCOOCOE
C.OOOCCCE
c.
c.
0.
0.
0.
0.
0.
•" ' — o.
c.
c.
0,
c .
• c.
c.
0.
0.
0.
0.
0.
c.
c.
OOOCOOE
OC2000E
OOOOCOE
OOOOOOE
OOOOOOE
OOOOOOE
OSJ030E
200000E
OOOCOOE
OCOCCOE
0000. OE
OOCOC'CE
OCOCCOE
0000-OE
0 0 2 G C 0 E
OOOOCOE
ooooaoE
OCCOCOE
OSfOCOE
OOOOOOE
ooccrcE
CCOOCOE
00
CO :
oo
00
00
00
00
oo - •
00
00
co — ~
00
00
00 '
00
00
?o —
CO
00
oo 	
no
00
oo
00
00
cc " 	
CO
20
CO
CO
00
co --- -
00
00
CO
CO
00
0
• o
0
.OOOOOOE
.OOOOOOE-
.OOOPOOE
00
00
00
0.266940E-01
0
c
0
0
r-t
c
c
0
0
c
0
c
0
0
0
0
0
0
0
0
0
c
0
Q
c
0
0
c
c
.683760E-01
.82251CE-01
.146769E
.213592E
•250CCOE
.285347E
.30S9COE
.315769E
.322751E
.344066E
.35S695E
.369663E
.37741CE
.385041E
.377410E
•365041E
.377410E
.369063E
.369863E
.344286E
,344C£6E
.351351E
.369 b65E
•369663E
.369663E
.369663E
.377410E
.377410E
.377410E
0.377410E
c
c
0
.377410E
.3774ICE
.377410E
00
CO
cc
00
CO
cc
oo
00
CO
00
00
00
00
00
00
00
00
00
00
CO
CO
00
CO
CO
oo
00
00
00
CO
oc
00
190345E 02 --UNUTES
                                                                                        M2504 LOADING
                                                                                        J3MS ACID/OK  C

                                                                                         0.206000E 00
                                                                                       ' 0.1S1530E CO
                                                                                         0.157061E CO
                                                                                         0.121500E 00
                                                                                         o.eea&boE-oi
                                                                                         C.6369eS£-Cl
                                                                                         0.507661E-01
                                                                                         0.3&5569E-2i
                                                                                         C.25352CE-C1
                                                                                         C.l6lfc!)6E-Ol
                                                                                         O.B66C67E-02
                                                                                         C.202475E-C2
                                                                                        -C.A21576E-02
                                                                                        -C.964649E-02
                                                                                        -0.14Q561E-C1
                                                                                        -C.1772b8E-Cl
                                                                                                       0.23561.-5C-C1
                                                                                                       0.2626b6E-Oi
                                                                                                       0.269716E-01
                                                                                                       0.315? JOE-Oi
                                                                                                       0.34E115E-01
                                                                                                       0.381C.J4E-01
                                                                                                       0.422512E-C1
                                                                                                      -C.470749E-C1
                                                                                                        • 50
                                                                                                      -0.656274E-;!
                                                                                                      -C.687628E-Oi
                                                                                                      -C.7i6c49E-01
                                                                                                      -0.7460S9E-C1
                                                                                                      -0.775269E-01
                                                                                                      -0.804479E-C1
                                                                                                      -0.8775C5E-0'.
                                                                                                                       RATE  ACIU
                                                                                                                       GX ACID/OM C-.XI.\.

                                                                                                                          O.OOOCOCt  00
-C.102»26:.-01
-0.9S865'-i-o2
-0.804'-l;>c-02
-C.613-'o»t-02
-0.509/74C-02
-0.408o6o--C2
 0.34- s2»c.-02
                                                                                                                         -0.302i:3tit-02
                                                                                                                         -0.24118^t-02
                                                                                                                         -0.19947 ^t-02
                                                                                                                         -0.167;9/;-02
                                                                                                                         -0.14605it-22
                                                                                                                         -0.124266C-02
                                                                                                            -0.16 /U9/L-02
                                                                                                            -0.16 I'j'S ^L-C2
                                                                                                             0.24iigjc.-02
                                                                                                            -0.241. feiL-02
                                                                                                           -0. 167^9 'L-02
                                                                                                           -0.16 /V9/S-02
                                                                                                           -0.16 '^9/c-02
                                                                                                           -0.l46C5i£-02
                                                                                                           •0. 146C5.C-C2
                                                                                                           -O.l46c5i--02
                                                                                                           -C.l46o5.t-C2
                                                                                                           -C.lfc6C-5iC.-OZ
                                                                                                           -0.i46C5.i-02
                  ;rF C- "Cli OECO'-'^OSiTION  =    -0.457S76E-02 AT    0.19C345E 02 MINUTES
                  vra*/;E =iTF OF ACID  0£CC"PCS IT I0\ UP TO ?C PERCENT ACID UTILIZATION  •
                                                                                            -0.931299E-02

-------
                                           	RATE OF SULFUK GENEKATION
                                                      BENCH SCALE
SG-?5
SPACF VELOCITY  =     0.116^37E  04  /HR
INEPT GAS FLOW  RATE  *       5SJO.OO SCC/"*IN
WEIGHT OF CARBONt  UNLOADED =       25.600  QMS
                                          LOADED
                  32.20 CMS
INLET PERCENT H2S  *       30.000
INLET MOLAR Has  CONCENTRATION  =
INLET SULFURIC ACID  LOADING  =
                           0.428571 VOLES H2S/MOLE INERT GAS
                         0.206000 GMS H2S04/GM CARBONt
FINAL OUTLET PERCENT  S'JLFUR  LOADING  ON  CARBON B      15.600
FINAL OUTLET SUL^U* LOADING  ON  CARBC\ »       0.196 GMS S/GM CARBON
INITIAL TEMPF9ATU9E »      '270.00  F		
MAXIMUM TFMPERATURF «      338.00  F
FINAL TEMPERATURE  =       318.oo F
                                                                            3 16 71
         PERCENT  H2S
                    PERCENT 502
 0.0
 2.0
 4.0
 6.0
 8.0
10.0
12.0
14.0
16.0
18.0
O.OOOOOOE
O.OOOOOOE
O.OOOOOOF
0.240000F
0.7600COF
0.148000F
0.20600CE
0.266000E
0.296000F
0.300000E
00
00
00
01
01
02
02
02 -'
02
02
O.OOOOOOE
	 O.OOOOOOE
O.OOCOOOE
U.'JUOOOOt
O.OOOOOOE
O.OOOOOOE
O.OOOOOOE
-- - C. OOOOOOE
O.COOOOOE
O.OOOOOOE
00
00
00
00
00
00
00
00
00
00
PERCENT C02
                                      O.OOOOOOE 00
                                   	O.OOOOOOE 00-
                                      0.OOOOOOE 00
                                      O.OOOOOOE 00
                                   	0.0000'JOE 'JO
                                      O.OOOOOOE 00
                                      O.OOOOi-'OE 00
                                   	OiOOOOUOE -JO
                                      O.OOOOOOE 00
                                      O.OOOOOOE 00
MOLAR CONC H2S
H2S04 LOADING
GMS ACI-/GM C
RATE
O.OOOOCOE 00
O.OOOOCOE 00
O.OOOOOOE 00
0.245901E-01
O.S22510E-01
0.173708E 00
0.259445E 00
0.362397E 00
0.420454E 00
0.428571E CO
0.2060JOE 00
0.1776&6E 00
0.1493/2E 00
0.1218 l£-01
0.7722 '3E-01
0.6322iSE-Ol
0.5544V2E-01
0.5299»2E-Ol
0.527270E-01
O.OOOCO-- 00
•»0«14i V6'^-01
-0. 14A ij6--<^-01
-0« 13i-!'41-'--01
-0«114-9?^-01
-C.84ictt^'--02
~0.55i:=-6-"--02
-0.21c-j9w^-02
-0«268i2*'t-c3
0.00^-Ovw 00
A+t* «f
                                     0.773 f-

-------
                                                     RATE OF SULFUR GENERATION
                                                           BENCH SCALE
     SG-2*

     SPACE VELOCITY  «     0.992250E 03 /HR
     INERT GAS  FLOW  RATE «       309.00 SCC/MIN
     WEIGHT OF  CARBON*  UNLOADED *      16.000 CMS
                       LOADED
                   20*00 CMS
      INLET PERCENT  H2S *       30.000
      INLET MOLAR  H2S CONCENTRATION »
      INLET SULFUR 1C ACID  LOADING *
        0*428571 MOLES H2S/MOLE INERT GAS
      0.206000 CMS H2S04/GM CARBONt
     FINAL OUTLET  PERCENT SULFUR LOADING ON CARBON »      18.400
     FINAL OUTLET  SULFUR LOADING ON CARBON *       0.229 GMS S/GM CARBON
     INITIAL  TEMPERATURE *      270.00 F     ~  -
     MAXIMUM  TEMPERATURE -      321.00 F
     FINAL TEMPERATURE »      303.00 F
                                                         3 11 71
ro
      TIME      PERCENT H2S
       0.0    O.OOOOOOE 00
       2.0    O.OOOOOOE 00
       4.0    0.1600COE 01
       6.0    0.440000E 01
       8.0    0.820000E 01
      10.0    0.114000E 02
      12.0    0.154QOOE 02
      14.0    0.186000E 02
      16.0    0.196000E 02
      19.0    0.2020COE 02
      21.0    0.212000E 02
      23.0    0.234000E 02
      26.0    0.256000E 02
      28.0    0.268000E 02
      31.0    0.284000E 02
      35.0    0.300000E 02
      37.0    0.300000E 02
 PERCENT S02
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOCOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
 PERCENT C02
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
O.OOOOOOE 00
MOLAR CONC H2S
  O.OOOOOOE 00
  O.OOOOOOE 00
  0.162601E-01
  0.460251E-01
  0.893246E-01
  0.128668E 00
  0.182033E 00
  0.228501E 00
  0.243781E 00
  0.253132E 00
  0.269035E 00
  0.305483E 00
  0.344086E 00
  0.366120E 00
  0.396643E 00
  0.428571E 00
  0.428571E 00
H2SC4 LOADING
GMS ACID/GM C
           00
           00
           00
           00
           00
0.2C6000E
0.181864E
0.158187E
0.1358C6E
O.U5482E
0.974853E-01
0.820988E-01
0.695234E-01
0.586866E-01
0.434718E-01
0.34Q397E-01
0.260817E-Q1
0.173145E-01
0.131771E-01
0.919110E-02
0.739333E-02
0.739333E-02
      ACID LOADING «    0.205999E-01 AT    0.248757E 02 MINUTES
      RATE OF ACID DECOMPOSITION «   -0.278624E-02 AT    0.2487S7E 02 MINUTES
      AVERAGE RATE OF ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION »   -0.709168E-02
RATE ACID DECOMP.
CM ACID/GM C-MIN.

   O.OOOOOOE 00
  -0.12067SE-01
  -O.U6Q97t-Oi
                   -Q.844456E-02
                   -0.69419JE-Q2
                   -0.563J50E-02
                    C.449215t.-o2
                    0.34658 /t-32
                    0.237690E-02
                    C.175647E-02
                    O.OOOOOi-E  OC
                    O.OOOOOOE  00

-------
                                                                     RATE OF SULFUR GENERATION
                                                                           BENCH SCALE
                  -  SG-23

                     SPACF  VELOCITY *    C.100654E Oft  /MR
                  -  :*E»T  GAS FLOW 9ATIT *       155.00  SCC/vlN
                     v.'FK'MT Cc CARBON. UNLOADED  *        7.9»0 G«S
                                                                        LOADED
                                                                                       10.00 CMS
                     INLET ocqcci,T _2s -      30.COO            ••  —	•-••  •-  	  --- •
                     INLET WOLAS H2S CONCENTRATION =    0.428571  «OLES H2S/MOLE INERT GAS
                     INLET SULPU"?IC ACID LOADING "    0.206000  GKS M2S04/GM  CARBON.

                     PP.AL CUTLET = E = CE',. SULF'JS LOADING ON  CARBON «       20.720
                     FI'.AL 0'JTL£T S'JL^L". LOADING ON CARBON «       0.260 CMS S/GM CARB3N
                     INITIAL TE"P£RAT'J'S »      270.00  F      '   	— -----
                     MAXlvu* TE''3E'?ATU'fr =      330.CO  F
                     FINAL TEvt>ERAT-j=£ •      320.OC F
           3 10 71
OO
TIVE
0.0
2.0 •
4.0
e.o
10.0 --•
17.0
14.0
16.0
18.0
20.0 .
2?.0
24.0
26.0
2? . 0
3C.O
32.0
34,0 -
n f ft
Jc . 0
3f .0
40.0 "•
44.0
46.0
-50. 0 -
53.0
56.0
'59.0 —
62.0
65.0
PERCENT H2S
O.OOOOOOE 00
O.tJOCOOE CO
0.1B4COOE 02
C.192000E 02
0.192COIE C2
0.1 92 CO
c.is-cc
C. 17400
0.15SCC
o.iseoo
C.:960U
c.2i-;:
C * 2 1 6 0 Z
*"" 2 1 ** " n
0.234::
0.214C3
C9 "a "• ^ •*
. / 1 -J - *•
0.256"
0.2361C
0.23600
c.233:o
0.24-CC
0.25230
E 02
E 02
E S2
E 02
E 02
E C2
E C2
E 02
c f\2
E 02
E 02
E C2
r ^9
. u£
c 02
E C2
E 32
E C2
E C2
E 02
C.263C30F 02
C.270COCF C2
C.274rCDE 02
0.2">4COOE 02
PERCENT 502
O.OOOOOOE
- O.C30300E
O.OOOOOCE
0.000003E
0.030000E
O.OCOOOOE
O.OOOOCCE
O.OOCCOCE
O.OCC30CE
3.3C3C30E
c.occ3":oE
0.303C30E
C.303700E
f* r* ^, n — ft ^i —
S.SOO:OCE
O.C030COE
n o .-\ • ,~\ A '\ c
C . u w ^ o u v ^
/> »>A«^/N^-^
'. • u J ^ J J w'C
3. 003CC CE
C< 00><003E
O.OO;OOOE
O.OCCOOCE
- G.503033E
D.COCOOC'E
" O.OOOOOOE
OlOSS'OCc
:.300000£
00
00
00
00
CO
00
00
00
00
'.'3
uO
00
CO
r>"
00
30
00
AH
uu
00
S3"
00
CO
CO
00
00
oo
cc
so
PERCENT C02 MOLAR CONC H2S
0.
• '0.
0.
COOOOOE
OOOO'JCE-
COOOOOE
O.OOOOOOE
	 — o.
0.
0.
	 o.
0.
0.
• — c.
0.
c.
0.
0.
c.
0.
.
0.
— •• — o.
0.
c.
	 o.
G.
3 .
0.
0.
0.
OOOOOOE'
OOOOOOE
3000C3E
COCC-JOE
OOCOOOE
COOOOOE
COC303E
030CUOE
OOCOOOE
C300COE
030CCOE
OOOO'JOE
030030E
,T"Jf> "* -'* AF
U JU— \- v/C
OOOOwOE
OOCCiOE
OOCOCOE
OOOOi-OE
OOOOC'.OE
OOOOOOE
OCOOJCE
OOOOv-OE'
OOOOuOE
OOOOOOE
00
CO
00
00
oo—
00
00
03 	
00
00
oo 	
00
00
CO " — "
00
00
co 	
o *\
•J U
00
co 	 •
00
CO
00
30
CO
00
00
00
3.000COOE
00
0.401606E-C2
0.225490E
0.237623E
0.237623E
0.237623E
0.225490E
C.210S53E
0.21951IE
0.231527E
0.243781E
C.2722-64E
C.278772E
0.278772E
0.256281E
0.272264E
0.27B772E
07Q fc 7 1 1 ~
*t?D 'WA^
0.344086E
0.308900E
0.33890CE
0.312335E
0.329787E
0.336b98E
0.351351E
0.369S63E
0.377410E
0.37741CE
00
00
CO
00
CO
CO
00
CO
03
00
00
CO
00
00
00 ~
nf>
UU
00
30
00
CO
CO
00
CO
00
00
oc
H2S04 LOADING
G"S ACIO/GX C
0.206000E 00
0.131716E CC
0.163854E OC
0.1414^4? 00
0.1305;>4E 00
0.1196B5E 00
0.1084/OE 00
0.964S75E-01
3.843343J-01
0.727762E-01
0.619063E-01
0.522COCE-31
0.434!, ,'SE-Ol
C .3496C3E— 01
0.257529E-01
O.l64403£-C'i
0.77279CE-32 "
»n 5~5Tri.c-.ra
O titJc i L*»!l v .*
-0.632314E-C2
-0.121438E-01
-0.257662E-D1
-0.3Z4327E-C1
-0.44722sE-Oi
—0 .52fi50oE— 01
-0.6006"4E-C1
-0.65c:676E-Oi
-0<"355£3E-Ol
-C.74926SE-C1
RATE Ado ^tCOi'.J.
G.»; ACID/CM C-XJ,,.
O.CCO^OOt 00
" -0.12063^-01
-0.57S014L-C2
— 0.54-3'»7*t-c2
-0.54J47>L-02
-0.54347*^-02
-0.576vl«-i-02
-0. 62024411-02
-0.59'-02 = t-02
-3.56oo3it-02
-0.526» = -.t-02
-0.444t)8pt-02
-C.426J6it-C2
™fi ii. 7 A *ftir"*O?
-o!490i7>£-02
-C.444c8it.-02
-0.426;6i--C2
-0.24U464L-02
" -O.J4C,uC'l--02
-0. J4060'£.-02
-3.333=3.^-32
-C.2oll6At-C2
-0.260>2»t-32
-0.219 '3at-02
-C.16709/i-02
-C.l4ibl;t-32
-3.l4iifclac-C2
                    ACID  LOADING =    C.205999E-01 'AT     0.311104E  02 MI.NUTES
                    PATE  Oc  «CID :ECOVCOSIT!ON »   -C.465116E-02  AT    0.31110'E 02 MINUTES
                    AVE°AGE  ^ATE Cc ACJ3 Drr:'-'POSIT lOV U°  TO  90 PERCcNT"ACIO UTIT.IZA" ION =
-0.571293E-02

-------
                                                                     RATE OF SULFUR  GENERATION
                                                                      -	 BENCH SCALE
                    SS-?1

                    SPACE VELOCITY »    0.10<,59BE C
K>
VQ
Tf-'E
0.0
?.o
''.0
6.0
P. 5
11.0
13.0
15.0
1 7 . 0 - - -
19.0
21.0
22.0 •
25.0
?7.C
29.0
31.0
33.0
• 35.3
37.3
30. c
^ 1 • C
**"'*«
51.3

5"". 3
• c c . ^
61.0
O.OOOOOOE
0.1<>OOCOC
0.19<.COCF
C.2C630CE
C.2130Cr.F
0. 2?**CCOE
C.216000E
0.2C2300F
0.19»COO?
0.2C2033F.
C'.2?7330F
0.223333F
C.23S003E
0,2'T-030E
0.2'.B303E
C.2'-53C';E
3.25'-f)0'JE
0.203003E
C.2620COF
3.2h?OJ'-F
3.262"00C
c!2700^F
?:2~o3lE
C.2?6000F
C.290000F
C.2^^000r
0 . 3 ? 0 0 C '• E
OC
02
02
02
02
02
C2
02
02
02
C2
02
02
C2
02
C2
02
02
02
02
02
32
02
02
n *
vV
C2
32
0?
02
PERCENT 502
0.
0.
0.
0.
c.
0.
0.
0.
OOOOOOE
OOOOOOE
OCOOOOE
COOOO'JE
OOOOOOE
3033COE
C33300E
OOOOOOE
o.ooaoooE
c.
0.
0.
c.
0.
0.
c.
0.
0.
0.
0.
0.
Oi
3.
0.
0.
0 •
o.
0.
2,
1^
c.
0.
3333 3CC
3C303CE
C00003E
3 C C 3 3 C E
OOOOOOE
OOOOCOE
03303CE
OCOO~OE
03330CF
00333 OE
030000F
30300CF
^ f\ A f> ^ f* jT
OOVOCCE
05000 OH
OCU33CE
00303CE
scjoccE
ccom-E
OOOOOOE
0003C!'E
3C333CE
OC03"'.'E
00
00
30
00
00
00
00
03
00
CO
00
CO
30
03
30
03
00
00
oc
CO
03
00
30
03
00
OC
03
00
30
00
00
CO
0
0
	 o
0
ft
. . Q
0
0
— 	 c
0
0
c
0
0
	 C
c
PERCENT C02 MOLAR CONC M2S
.OOOOOOE
.OOOOOOE
.OOOOOOE
.0030UOE
. OOCOoOE
. OOOOOOE
.OOOOJOE
.OOOO'-JOE
.OOOOUOE
. OOOO'JOE
.0000-CE
. OOOO'JOE
.0030JCE
.0300UQE
.OOOOCOE
.0000 JOE
C.COOO~OE
0
0
0
	 c
c
r<
' 0
0
0
._ £
0
Q
0
0
c
.ooaoooE
.OC30JOE
,C300,;OE
.0000 OOE
.COOOJOE
.CCOOJOE
.OOOOJOE
•OOOOJOE
.U030UOE
•30UOJOE
. OOOO'JOE
.OOOO'TOE
.3COCJCE
.OOOOJOE
.O'iCOi'OE
00
oo
oo - -
oo
i>0
,ao 	
JO
00
•yQ 	
JO
JO
30 	
JO
JO
30 	
UO
JO
00" 	
JO
JO
'00
DO
'JO
00
00
JO
oo 	
30
00
CO
JO
1/0
O.OOOOOOE
0.162790E
0«2'>069'tE
0.259i't5E
0.265822E
0.288659E
0.275510E
0.253132E
0.2'-6BB2E
0.253132E
0.2B2051E
0.295336E
0.3C3903E
0.322751E
0.329787E
0.329787E
0.3<.C''82E
0.3'.770SE
0.355313E
0.355C13E
0.355013E
C.369863E
C.369663E
0.377410E
0.377410E
0.3950'tlE
0.392757E
0.403560E
O.^OE'-SOE
0.^16A33E
3.^28571£
O.'.?f 571E
00
00
00
oo
00
00
00
00
00
03
00
00
00
00
00
00
00
00
00
00
00
CO
03
00
00
00
03
oc
00
cc
CO
00
                                                    M2S04 LOADING
                                                    GMS ACI3/GM C

                                                     0.2063JOE 00
                                                     0.165L-02


                                                                       -0.1511'3'.t.-o2
                                                                                                                                    wGwE. 00
                                                                                                                                    JO.- oo
                       :3 LO'Di-.r, =     3.205990^-31 />r    c.<-662ieE 32 «INUTES
                        E C= ;C1D SECCVDOS: r!0\ =   -0.155761E-02 AT     0.<»66218E  02  MINUTES
                       E'AJE si'r OF  ACIC  OrCO-'''»OSlTiO>: u-> TO 90 PERCENT  ACID UTILIZATION «
                                         -0.373*63E-C2

-------
                                                           KATE OF SULFUR GENERATION
                                                                 BtNCH SCALE
                                     1 71
           SG-<»3
           SPACt VELCClf'Y =   " "b". 309191E  03 /HR
           INERT GAS FLOW RATE =      7064.00 SCC/MIN
           WEIGHT UF CARBONi UNLOADED =     1179.000 GMS
LOADED
1486.00 GHS
           INLET PERCENT H2S =       29.700
           INL§T_MOL_AR H2S CONCENTRATION  =     0.422475 MOLES H2S/MQLE INERT GAS
           INLET suLfURIC ACIO LOADING""«     o.i366oo GMS H2S04/GM~CARBUN,

           5.INAL OUTLET PF.RCENT  SULFUR  LOADING ON CARBON =	21.080	
          "FINAL OUTLET SULFU«" LOADING  ON CARBON = "     0.266 GMS  S/GM CARBON
           INITIAL TEMPEKATURE =      290.00 F
           MAXIMUM TEMPERATURE =      3*0j-?ll_f	
           FINAL TEMPERATURE =     ""320^00 >    .            "      ~      ~~
to
U>
o
TIME
0.0
10.0
20.0
30.0
40.0
50.0
60.0
70. 0
60.0
90.0
100.0
110.0
ACID
RATE
PERCENT H2S
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.270000E 02
0.290000E 02
0.29^0006 02
0.297000E 02
0.280000E 02
PERCENT S02 PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
LOADING = 0.136000E-01 AT
OF ACID DECOMPOSITION = -0.
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.331655E 02 MINUTES
3690596-02 AT 0.331655E
MOLAR CONC H2S
0.0
0..0
0.0
0.0
0.0
0.0
0.0
0.369863E 00
0.40B451E 00
0.
-------
                                                          RATE OF SULFUR GENERATION
                                                                BENCH SCALE
          SG-44

          "SPACE  VELOCITY  =    0.309191E 03 /HR~	
          INERT  GAS  FLOW  RATE  =     7064.00 SCC/KIN
          WEIGHT  OF  CARBON,  UNLOADED =    1179.000 CMS
    LOADED
                               1486.00 CMS
           INLET  PERCENT  H2S =      29.000
           INLET  MOLAR  H2S CONCENTRAT ION_ =
           INLET  SULFURIC ACIO LOADING =
 __ 0.408451  MOLES H2S/MOLE _
"0.136000 CMS H2S04/GM CARBON,
                   GAS
                                      9  2 71
          FINAL  OUTLET  PERCENT SULFUR LOADING ON CARBON
          FINAL  OUTLET  SULFUR LOADING"ON CARBON =
          INITIAL  TEMPERATURE =      250.00 F
          _MAXIMUM  TEMPERATURE =	355.00 JF	
          FINAL  TEMPERATURE =""  " 310".00 F  "
       22.040
0.278 GMS S/GM CARBON
           THE  "    PERCENf H2S
to
u>
             0.0  "  0.0
            10.0    0.150000E 01
          _20.0	0.130000E_01
            30~.0    6.930000E" 01 "
            40.0    O.ll^>000t 02
            50.0    0.145000E 02
          ""60.0    0.270000E 02
            70.0    0.285COOE 02
            80.0    0.290000E 02
           "90.0 "   0.293000E 02~
           100.0    0.290000E 02
           110.0    0.29COOOE 02
PERCENT 502
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
OOOE-01 AT 0.387428E
ION = -0.246304E-02 AT
PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
o.o :•-'
0.0
0.0
0.0
0.0
02 MINUTES
0.387428E
MOLAR CONC H2S
0.0
0.152284E-01
OM31712E-01
0.102536E 00
0.129943E 00
0.169591E 00
0.369863E 00
0.398601E 00
0.408451E 00
0.414427E 00
0.408451E 00
0.408451E 00
02 MINUTES
H2
GM

^i
»
— i
-l
-l
-i
— i

                                     H2S04 LOADING
                                     GMS ACID/GM C
                                                                         ~ACI"D OECOMP".
                                                                    GM ACID/GM C-KIN.
                                       0.100984E 00
                                       0.665441E-01
                                       0.359172E"-01
                                       0.103907E-01
                                      -0.122069E-01
                                      -6.243253E-Or
                                      -0.264410E-01
                                      1°-JL26 871 2E- 0 1_
                                      -0.266lOiE-01
                                      -0.263491E-01
                                      -0.263491E-01
                                                                        0.0
                                                                       -0.343504E-02
                                                                       -0.345301E-02
                                                                       -0.2672366-02"
                                                                       -0.243294E-02
                                                                       -0.208659E-02
           ACID LOADING =    0.:
           RATE OF ACIO DECOKPO!	  		          	
          "AVERAGE RATE OF ACID DECOKPO'SITION UP TO 96 PERCENf ACID UTILIZATION =   -o.302348E-02
                                                                        0.860399E-04
                                                                        0.0
                                                                        6.52205~9E-64~
                                                                        0.0
                                                                        0.0

-------
OJ
                                                           RATE  OF  SULFUR GENERATION
                                                                 BENCH SCALE
                                       9   2  71
          SG-45
          SPACE VELOCITY  =     0.528427E 03~~/H~S
          INERT GAS  FLOW  RATE  =    11827.00 SCC/MIN
         JUL!GHT_PF"  CARbO.M,  UNLOADED =    1151 ..Oqo. QMS
    LOADED
•1451.00 CMS
          INLET PERCENT  H2S =      30.000
          INLE_L_MOLAR JH2S  CONCENTRATION^	0.428571  MOL|S_M2S/MCIL£ INERJ GAS
          INLET SULFUR 1C ACID' LOAD ING" =    O."l3600~0  GMS~ H2S04/GM CARBON",
         JF INAL_ OUTLET _f>ERCENT SULFUR LOADING DN CARBON  «
          FINAL OUTLET  SULFUK LOADING ON CAiRBON =
          INITIAL TEMPERATURE =      260.00 F
         _MAXIMUM TEHPERATURE_=_	315.00_F	
          FINAL TEMPEKATURE  =      300.0b"F
       20.400
0.257 GMS S/GM CARBON
TIME
" b.o
10.0
20.0
30.0
40.0
50.0
ACID
*ATE
PERCENT H2S
0.0
0.100000E 01
0.185000E 02
0.270000E 02
0.300000E 02
0.300000E 02
PERCENT S02
0 = 0
0.0
0.0
0.0
0.0
0.0
LOADING = 0.136000E-01 AT 0.2641306
CF ACID DECOMPOSITION = -0.164731 E-02 AT
PERCENT CC2
0.0
o.o .' ;:,. ,
0.0 -• •"••- •••-.
0.0
0.0
0.0
02 MINUTES
0.264130E
MOLAR CONC H2S
0.0
0.101010E-01
0.226994E 00
0.369863E 00
0.428571E 00
0.428571E 00
02 MINUTES
H2S04 LOADING
GMS ACID/GM C
0.136000E 00
0.725501E-01
0.261037E-01
0.660623E-02
0.220852E-02
0.220852E-02

RATE ACID OECOMP.
GM ACID/GM C-MIN.
0.0
-0.626933E-02
-0.301994E-02
-0.879543E-03
0.0
0.0

          AVERAGE RATE  OF^ACID DECOMPOSITION UP TO 90  PERCENT  ACID UTILIZATION
                            -0.391689E-02

-------
                                                           RATE OF SULFUR GENERATION
                                                                 BENCH SCALE
           SG-46
           SPACE VELOCITY'S     o.930io7E 02 YHR	""
           INERT GAS FLOW  RATE  =      2392.00 SCC/MIN
           HEIGHT OF CARBON,  UNLOADED =    1124.000 CMS
                  LOADED
1417.00 CMS
           INLET PERCENT  H2S  =       18.000
           JNLET MOLAR  H2S  CONCENTRATION =_
           INLET SULFURIC ACID  lOADING" ="
_ °-2A9!1.2  MOLES  H2S/MOLE JNERT_GAS_
0.136000  GMS  H2S04/GM CARBON,
           FJNAL OUTLET  PERCENT  SULFUR k°ADI_NG_ ON CAR30N
           FINAL'OUTLET  SULFUR LOADI.NG'ON CARBON =
           INITIAL  TEMPERATURE =      255.00 F
           MAXIMUM  TEMPERATURE =	3
-------
                                                          RATE OF SULFUR GENERATION

                                                                BtNCH SCALE
                                                                                        1 71
          SG-47


          SPACE  VELOCITY =    0.7749276 03 /HR
          INERT  GAS FLOW RATE =    16584.00 SCC/MIN

          _*l£iGHl_UF CAR3QNt_UNLpADEi}_5	1126.000 CMS
                                                   LOAD£0
1419.00 'CMS
           INLET  PERCENT H2S =      27.300

           INLET  HULAR H2S CONCENTRATION =
           INLET  SULFURIC ACID LOADING =
                                    0.375516 HOLES H2S/HQLE  INERT GAS
                                  0.136000 &MS H2SO4/GM CARBON.
JLINAL__OUTLET_ PERCENT SULFUR LOADING ON CARBON
 FINAL OUTLET "SULFUR LOADING ON CARBON =
 INITIAL TEMPERATURE =      250.00 f
_MAXIMUM JLEMPERATURE_^	385.00 F	
 FINAL TEMPERATURE =      310.00 F
                                                                20.44Q
                                                         0.258 GMS S/GM CARBON
U>
TIME
0.0
10.0
_ 20.0
30.0
40.0
50.0
PERCENT H2S
0
0
0
0
0
0
.0
. 182000E
.Z27000E
.260000E
.266000E
.273COOE
02
02
02
02
02 _.
PERCENT S02
0
0
0
0
0
0
.0 ,
. 0
.0 . . ...:.;,-. .
.0
.0
.0
PERCENT C02
0
0
0
0
0
0
.0 ;
.0 :••£-. ..::••-:;•
.0 , ,.-;^"-. ••::"'
.0
.0
.0
MOLAR CONG H2S
0.0
0.222494E
0.293661E
0.351351E
0.362398E
0^3755166
00
00
00
00
00
H2S04 LOADING RATE ACIt) iJECOKP.
GMS ACID/GM,C GM ACID/GC C-KIN.
0.136000E 00
0.792515E-01 '•;
i0.54.0331E-01
0.426499E-01
0.386470E-01
0.372385E-C1
0.0
-0.328595E-02
-0.175773E-02
-0.518fc98E-03
-0.281692E-03
0.0

-------
                                                           RATE OF SULFDK GENERATION
                                                                 BENCH SCALE
                                                    9  2 71
           SG-48
U>
           SPACE VELOCITY  =     0.101530E  04 /HR
           INERT GAS FLOW  RATE  =     22383.00 SCC/KIN
           •.EIGHT OF CARBON,  UNLOADED *     1134.000 CMS
                 LOADED  -
1429.00 GMS
           INLET PERCENT H2S  =       33.800
           INLET'MOLAR H2S  CONCENTRATION f
           INLET "SULFURIC AC 10  LOADING ~="
_ 0.510574 HOLES H2S/MOLE  INERT  GAS
0.136000 GMS H2S04/GM CARBON,"
           FINAL OUTLET  PERCENTJSULFUR  LOADING ON CARBON =
           FINAL OUTLET  SULFUR LOADING"ON CARbON =
           INITIAL TEMPERATURE =       250.00 F
           MAXIMUM TEMPERATURE, f	385.00_F	
           FINAL TEMPERATURE  = ~    290.~00 F
                     19.080
             0.240  GMS  S/GM  CARSON
           TIME
             0.0
             10.0
PERCENT H2S
0.0
0.219000E 02
0.324000E 02
PERCENT
0.0
0.0
0.0
0.338000E 02 0.0
IING = 0.1360COE-01 AT
S02 PERCENT C02
0.0 V
0.0
0.0
0.0
0.142038E 02 MINUTES
MOLAR CONC H2S
0.0
0.280410E 00
0.479290E 00
O.510574E 00
H2S04 LOADING RATE
GMS ACID/GM C GM I
0.136000E 00
0.294148E-01 ' -
-0.820515E-02 ' -
-0. 127066E-01
                                                                    RATE  AC'ID DECOMP.
                                                                    GM  ACID/GM C-MIN.
             30.0
            RATE  OF  ACID DECOMPOSITION =   -0.421767E-02 AT    0.142036E 02 MINUTES
            AVERAGE  RATE OF ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION =   -0.591159E-02
                                                                        0.0
                                                                      -0.662369E-02
                                                                      -0.900292E-03
                                                                        0.6

-------
                                                         RATE  OF  SULFUR  GENERATION
                                                               BENCH  SCALE
                                                   9  2 71
         SG-49
         SPACE VELOCITY =    0.181932E 03  /HR
         INERT GAS FLOW RATE =      2*32.00 SCC/MIN
         WEIGHT OF CARBQNt UNLOADED =     1118.000 CMS
                 LOADED
1409.00 GKS
         INLET PERCENT H2S =       57.000
         INLET MOLAR H2S CONCENTRAJION_*_
        "INLET SULF-URIC ACID LOADING  =
  1.325531 MOLES H2S/HOLE INERT GAS
0.136000 GMS H2SOWGH CAROON,
        _fJNAL_OUTLeT _PE_RCENT SULFUR. LOADING  ON  CARBON
         FINAL OUTLET SULFUR LOADING  ON CARBON =
         INITIAL TEMPERATURE =       250.00 F
         MAXIMUM TEMPERATURE 5	385.00 J:	
         FINAL TEMPERATURE =      275.00 F
                    16.360
             0.206 GMS S/GM CARBON
U>
         TIME
           0.0
          10.0
         _2p.«P_
          30.0
          38.0
         AVERAG!
PERCENT H2S PERCENT S02
0.0 '-'-' 0.0
0.0 0.0
0.220000E 02 0.0 .
0.325000E 02 0.0
0.<»50000E 02 0.0
PERCENT C02
0.0
0.0 :
o.o ;•'...-. .'•;
0.0
0.0
MOLAR CONC H2S
0.0
0.0
0.262051E 00
0.481481E 00
0.818182E 00
H2S04 LOADING
GMS ACID.'GM C
0.136000E 00
0.939578E-01
0.56388^E-01
0« 26
-------
                                                          RATE OF SULFUR GENERATION
                                                                HtNCH SCALt
                                                                                                   2  71
          SG-51

          SPACE VELOCITY  =     0.105J47E  03 /HR
          INFRF r,AS FLOW  KATE  =      2446.00 SCC/MIN
          ViblGHT OF tARBONt  UNLOADED =     1194.000 GMS
                                                    LOADfcO
_L505. 00 _GMS	
          INLET PERCENT  H2S  -       34.500
          JNLET MOLAR  H2S  CONCENTRATION =
          INLET SULF4JRIC ACID  LOADING =
                                    0.526718  MOLES  H2S/MOLE  INERT GAS
                                  0.136000 GMS  H2S04/GM  CARBONf
_FJNAL_pUTLET PERCENT SULFUR LOADING ON CARBON  =	13^840
 FINAL OUTLE'T"SULFUR" LOADING ON CAR"BON =
 INITIAL TEMPERATURE =      235.00 f
"F INAL TEMPERATURE"~»      2io.Fo "F"   ~  ~~
                                                         0.174 GMS S/GM CARBON
LO
TIME
0.0
10.0
20.0
30.0
40.0
50.0
60.0
: 70.0
80.0
90.0
100.0
110. 0
120.0
130.0
140.0
~"ibo.o
160.0
170.0
IBO.O
190.0
200.0
210.0
PERCENT H2S
0.0
0.0
0.0
OvO
0*0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.540000E 01
0.188000E 02
0.235000E 02
0.360000E 02
0.310000E 02
0.345000E 02
0.345000E 02
0.345000E 02
PERCENT S02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0 __
0.0
0.0
0.0
0.0
0.0
0.0
0.0
PER(
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
ENT C02 MOLAR CONC H2S
0.0
. •::-•-;,:•'•-.. ;- 0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.570825E-01
0.231527E 00
0.307190E 00
0.562500E 00
0.449275E 00
0.526718E 00
0.526718E 00
0.526718E 00
INUTES
H2S04 LOADING
GMS ACIU/GM C
0.136000E 00
0.120268E 00
0.104536E 00
0.888035E-01
0.730713E-01
0.573392E-01
0.416071E-01
0.256749E-01
0.101428E-01
-0.558928E-02
-0.213214E-01
-0. 370535E-01
-0.527856E-01
-0.685177E-01
-0.833973E-01
-0.948193E-01
-0.1025C6E 00
-0.105250E 00
-0.105872E 00
-0.1G7029E 00
-0. 107029E 00
-6.107029E 00
RATE ACID OECOMP
GM ACID/GM C-MIN
0.0
-0.157J21E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.157321E-02
-0.140272E-02
-0.881682E-03
-0.655691E-03
0. 106P76E-03
-0.231306E-03
0.0
0.0
" 0.0 "
           ACID LOADING =    0.136000E-01 AT	0.77802'>E 0;
           RATE OF ACID DECOMPOSITION - " -0. 1573^2IE-02 AT    0.778025E 02 MIMUTES
           AVERAGE RATE OF ACID UECtHPOS1TIUN UP TO 90 PERCENT ACID UTILIZATION *   -0.157321E-02

-------
         APPENDIX    A-11





SULFUR GENERATION EXPERIMENTAL DATA
                 238

-------
           -'OS-.! SuLJTJr. AMD SC-2 AZ^IYSES 01C  CAKBGN
             AS A FU:::YI.;IC D? IBS ?cs nux DSC-?
             / "•• O ~~ a TI   >   — .	•• „. -     .    -H  -•  _ _ _ \
             Vc2>  F fc.t   >o".; -^S ar.^.    0  -j  r.C;
IOTA.L SUIFuK AHD S02 AKA.LYSES  ON CARBON
  AS A FUuCIIOS OF SIK3 FOR Hull 3SG-8
  ( 325°? s.t  1C % H2S and   0 % H20)
i
i
Elapsed Ti.-e ,
=in. 'IOC
Total Sulfur, j SOg Analysis, * 1
^ ! Its. S02/100 TDS. C
C j 5-3 i 14.63
r - ' ' "• -, -, i
C . ~ ' ; - i-
! ?'-• ; ^-3 i 17.6
i;c

n 0 r
7-6
7.2
18.2
16.4
i 15-' 3.5 i 13-95
: 175 : C.4
• ^ r
235 9-6
to
U)
VO




260
230
~-'0
330
^--^
;.cu
390
425
450
1^90
1
9-1
9-7
9-4
1C. 4
11.8
10.5
11-5
—
—
12.21
11.18
9-4
8.56
7.5
6.4
5-52
^-75
4.1
3-56
3-12
2-95
*• Meaz-orei SO; evolution oy H202  corubb:r.g when careen
  heated  LO 1000°F
Elapsed Tice,
tain. /ICO
0
20
1*0
60
30
100
120
iko "
160
180
200
220
21)0
260
280
300
320
3l+0
360
380
ItOC
420
1*40
1*60
1)80
500
Total Sulfur,
%
6.48
7.40
8.00
7-92
8.44
8.72
9.12
9-76
9.80
9-6
10.04
10.48
n.32
11.48
3J..68
11.96
12.4
12.60
13.08
11.6
13.4
13.3
13-68
13.4
13.96
14.52
S02 Analysis,
Ibs. SOp/100 Ibs. C
14.77
17-53
19-57
19-36
16.95
16.00
14.38
13-75
12.85
11.26
9-93
9-96
7.80
6.46
5-54
5-19
4.75
3-73
2.94
3-27
3-03
2.82
2.64
1.54
2.27
2.73

-------
                    Cr-l:-L  S'Jui?. >.;._/  S02 AlilYSSS C"..'  CA.KECii

                     AS A JLI;CIIO:; o?  II:-E ?CR ?.~j~.\ rs^-9
15
                                                  0 •; X2C)
TOTAL SULFUR AKD S02 ANALYSES  OK CARBON

  AS A FUNCTION CF TE-E FOR ROT DSG-10


  ( 325 °F at 20.8$ HgS and   0  $ E2o)
to
4>
O
-in. /IOC
.

-
*"
1 ^
\ '-'
; 55
75
95
•» -, c
I ^-*>
i i>5
1 175
200
220
260
520
550
275
4oo
425
450
475
500
Tccal Sulfur,


•7 " -
I . v,'^
7.&0
S.32
8.08
9.c4
9.16
9-88
10.20
1C. -2
10.52
12.0
12.76
13-60
14.04
14.23
14.08
14.60
14.52
14.60
14.76
15.20
SCp Analysis,
Its. 30? ICO Its. C


** — r^7
17.4
1S.T3
16.28
16.96
14.48
12-73
12.53
11.04
9-73
8.57
4.47
3-39
3.70
3-13
2.98
2.58
2.97
2.96
2.64
3-06
Elapsed. Tiae ,
min . /ICO
0
10
30
50
75
100
225
150
175
200
225
250
275
300
325
350
375
400
425
450
475
500
Total Sulfur,
*
6.0
7-7
8.5
8.7
9-8
9-6
io.4
11.4
11.5
12.5
13.5
13-7
14.3
15-3
14.0
15.4
14.1
14.9
15-2
15-4
14.6
14.8
302 Analysis
Ibs. S02/100 Ibs. C

15-1
18.3
19-6
17.5
13-9
11.5
9-26
9-14
8.02
6.64
5-23
3-97
3-58
2.70
2.76
2.35
2.S3
2.38
2.68
2.65
2.39

-------

T03VL SUJVFUR AM) 302 AIK.LYSSS CN CA.B30N
  AS A ?-JI\CTIOH OF 3II/S FO?. EUII DSC-12

  ( 315°?  at  5-3$ H2S and  30 %

Slapsed Ti™e, ! -CTs.1 Sulfur, ZC-.- Analysis
„-•„ '"0'^ ' ;'- ' "v>s. SCs'lCO loo. C
• ; t
• >-r - r * - : -,
1 <• , 1 - .- - — * —
ic ; E.S: i 18.76

*."'
! =z
i

11-1
O.lj
15.4
1C . 12 1- - 5
ic. :s
12.43 1
11. f-' 11-42
I —^ , 12. oO i 7-~~

t
150
175
N> 1 20C
+> 225
13-32
14.20
15.20
15.44
1-1 2?0 | 16. vO
6.69
5-36
3.92
2.86
2,50
275 I 15-50 2.765



325 16 . c
350
375
I }. -^f^
1 425
450


475
500
16.64
16.46
16.76
17.00
16.04
17.20
16.46
2.449
2.248
2.42
6.49
2.41
2.65
2.175
2.53
Elapsed Time,
min./lOC
0
15
22
to
70
100
125
150
200
250
275
300
Total Sulfur.
%
6.4
6.60
8.4
7.03
7-52
7-2
7-36
7-^
7-96
8.0
8.20
7-84
SOg Analysis
IDS. SC2/100 its. C
16.08
	
17.30
16.8
17.04
17.34
17.48
17-74
18.8
17.28
17.48
16.80

-------
TOTAL SULFIG. AID C02 Al^LYSES 01' CA.-iQ:


  i 51:;F  it  5-3f; H23 ar.d  20 •;', >;2c)
TOTAL SUEF^ A:E 302 AIALYSES  oic CAI^D
  AS A FUHCTICH 0? TBS FOR RUN  DSC-i

              5-3-5 H23 and   1C£ :-I2o)

£i;in!/icr'
cf
! :
' C j 6.6t
1C ! c.20
S02 Analysj.3
Its. SC2/1CO 1'os. C

15.5
17-1
JO ! 7 .2,6 : lD.92

50 i 7-20
! 75 ! 7-12
I ICC ! c.OO
17-73
17.6
17. 6t
I :^r : 7--o ! 17.25
; 150

"75
N3 2CO
-P-
N>

225
2C0
• ~-~"^
! ~~^
''. 350


too
't25
•7 V" ' 17 £8
j . ~~r ^- 1 . '-'^
3. CO
7-2t
3.32
S.co
o.bO
17-99
17-73
17.93
17.9
15.68
? 0- ! -'5.68
8.12
8.20
6.8t
15- 3t
It. 32
It. 57
Elapsed Tims .
nin./100
0
25
ko
6c
75
100
125
150
175
200
225
250
275
300
325
350
375
too
1*25
t50
t75
500
Total Sulfur,
",j
(• ^

7.00
7.2t
7.12
7.52
7-36
7-12
6.96
7.2t
8.0
7.2
9-28
8.60
6.8
8.60
9.00
8.92
7-6t
7-72
7.36
8.68
9-6
S02 Analysis
Its. SOa/100 Its. C
18.15
l'^92
16.63
15. t3
20.3
21.1
18.0
17-3
17.63
18.2
15.65
15.2
13-35
13. 7t
Ik.kd
12.76
10.83
10.6
9-96
9-26
9-39
8.t7

-------
                    TOTAL SULFUR AJSD SC>2 ANALYSES OS CAHBOH
                      AS A FUNCTION OF TIM3 FOR HUN DSG-15
                                                                      TOTAL SULFUH AND SOg ANALYSES ON  CARBON
                                                                        AS A FUNCTION OF THE FOR RUN DSG-16
(275 °F at
                                       E23 and   0 %
(  275°F at
and
U>
| Zlapsed Tine,
nin./lOO
I 	 ,
0
15
30
50
75
100
125
15C
175
200
250
275
300
350
375
VOG
1*25
1*50
!*75
500
Total Sulfur,
/-'
6.12
e.kk
6.51
7.62
7.68
7.72
8.00
8.08
8.96
9-00
8.2
9.0
9.2
10.0
10.1
11.0
11.2
_11.2
, "l0.8
11.1
502 Analysis ,
los. SCto/'lCO Ibs. C
1
11*. 1
15-5
16.3
15-8
lit. 5
U.2
13.7
12.9
12.4
™
12.05
11.29
10.12
9.32
S.29
9.12
7-51
6.90
6.60
7-03
5-j 35
Elapsed Time,
min./lOO
15-
30
50
75
100
125
150
175
200
225
250
300
325
375
koo
1+25
450
U75
500
Total Siilfxir,
%
6.1
7. U
7.8
8.9
9.7
.10. ^
9-6
10.6
10.8
11.2
11.3
10.1
11. k
11.8
12.1
13.8
13.3
13.5
13.7
S02 Analysis,
Its. SQ2/100 Ibs. C
15; 80
15-19
13.75
12.21*
11.50
	
9.25
B,6k
7-73
7-^3
6.97
6.28
5-57
lj.75
U.W
^.99
3.1*3
U.31
3.37

-------
                    -CTA1  SULFy? A1C2 502 AlIAliSZS Oi: CA330K
                      AS A FuiiCTic:; :? :r~-z ?o?. ?:j.i 330-17

                      ( 2?5°F  at 25-4$ EgS and   0 % ;-;23)
TOIA.L SULFUR ACT S0£ AKALYSES ON CARBON
  A3 A FUNCTION OF TBS FOR RUN DSG-18

  !  325 °F at  5-0-p H2S and   0 % H20)
            Slapsea Tine,   I   Total sulfur,  !      302 Analysis,
              -in./ICO               *        '   Has. SCc/lOO  Its.  C
N)

0
20
40
s^ w
.
6. 84
	
15-23
—
9.6 10.99
9-1- ! 9-79
; 30 11.72 ! 7.5
j 125 i 11-25 6.47
150
175
225
250
275
3.00
325
350
375
400
425
450
475
500
12.60 5-68
13-52 4.36
14.12
13.76
13.54
5.6
4.38
4.86
15.0 : 4.9
14.48 3.74
15.0 ! 3-93
15.2
15-32
14.68
15-72
3.24
3.64
4.97
5.28
14.8 5-6
15.36 5-19
Elapsed Tine ,
min./iOC
0
20
40
60
30
100
125
150
175
225
250
275
300
325
350
375
i|00
1+25
450
475
500
Total Sulfur,
%
6.7
6.6
6.8
7-1
8.2
7-3
5.8
6.8
7-1
7.1
7.2
3.1
8.8
9.8
9A
—
—
___
—
—
"••"
S02 Analysis
Ibs. S02/1CO Ibs. C
15.1
15-7
16.44
16.0
15.0
14.5
13-1
12.0
8.75
8.45
8.62
—
6.57
5.6
4.95
4.66
4.32
4.06
3-7
4.36
3-93

-------
                     TOBi.Ii SULFUR AND S02 ANALYSES ON CARBON
                       AS A FUNCTION OF TIME  FOR HUH DSC-19

                       (  325"F at 9-1% H2S and   0  % H2C)
TOTAL SULFUR AHD S02 ANALYSES OK CARBON
  AS A FUNCTION OF TIMS FOR RUN DSG-80

  ( 325"? at 18.2$ EgS and   0 % H20)
N>
-P-
Elapsed Tine,
•»— - -V, / ~ f*f\
la^Ji . » .JLVW
0
j-5
30
50
Total Sulfur, |
ci i
8.5
6-9
S.O
7-9
75 " 8A
100 | 8.5
125
150
.L'f ^>
200
225
250
275
300
350
375
Uoo
^25
ir50
VT5
500
8.5
9-1
10.2
10.1
10,2
10.8
11.7
H-9
12.0
13-1
12.8
12.6
12.2
Z2..1
32.. 3
S02 Analysis
Ibs. S02/100 IDS. C
16.1
16.21
15-33
lit, 65
12.92
ll.C-7
9-25
7-96
7-52
6.22
if. 78
3-75
3.82
3^5
3-31
2.94
3-21
2.97
3-05
2.95
3-25
Elapsed Time,
min./lOO
0
15
35
65
100
125
150
175
200
250
275
300
325
350
375
425
if 50
VT5
500
_
Total Sulfur,
5-9
7.8
8.2
9.5
11.3
10-9
11-5
12.8
13-2
13.3
13. if
13.7
lif.5
13.5
13.3
13.lt
14. 5
13.2
14.5

S02 Analysis,
Its. S02/100 Its. C
15.0
l6.3
14.6
12.0
9-16
T.05
6.25
4.68
4.6
3-49
3.38
3.52
3.19
3.19
3.6l
4.03
3.48
2.99
4.13


-------
TOTAL SULFUR AJO) SO 2


  ( 325°? at  26.~:  EC
^jYSi.5 s^_\ CAR30I7
 ?0a BUS DSC-21

=id   C 5 K2C)
                                                                                              TOTAL SULFUH A3D S02 ANALYSES OH  CARBON
                                                                                                AS A FUNCTION OF TIME FC3 RUN DSG-22

                                                                                                (325 °F at 37-6£ H2S and   0
to
ilapsed Tide,
ain . /ICO
;
0
25
50
t '
i '^
! 3?
100
125
150
175
200
225
250
275
300
i 325
i 350
j 375
too
! t25
t50
t75
500
Total Sulfur, '. £0g Analysis,
;1 1 Ibs. SOg/iOO Ibs. C
7.6
6.t
10. '•*
11.3
12.3
12.6
15.5
T 5 £
13.9
it. 9
15-1
15-0
15.1
15-2
it. 7
15-2
15. c
15.0
15.3
15- 1
15 A
15.21
16.52
12.3
10.73 I
9-7
7-95
6.31
5.02
4.19
3.77
3.59
3.37
3.12
3.37
I'M
3.33
2.86
j 2.6
2.83
1.13
3-03 .
•Elapsed ?ine,
min . /100
0
20
t5
70
100
125
150
175
200
225
250
300
325
350
375
too
1*25
450
t75
500
To-jal Sulfur, .' SOg Analysis,
% | Ibs. S02/100 Ibs. C
6.t
8.0
9.1
11.6
It. 3
It. 2
lt.0
It. 7
15.0
15.3
it. 7
15.lt
It. 7 •
It. 7
It. 3
16.2
15.5
13.7
It. 2
15.1
15.03
13.39
9.37
7.12
t.35
t.05
t.2t
3-30
3.39
2.85
2.33
2.5
2.76
3.35
2.29
2.61
3.53
5-38
2.76
2.81

-------
                        APPENDIX A-12


              DETAILED RESULTS OF INTEGRAL RUNS
                                                         Page
 1.   Experimental Data and Results for Integral           248
       Run IR-1-4 (188 - 243 hours)

 2.   Experimental Data and Results for Integral           260
       Run IR-1-5 (246 - 262 hours)

 3.   Experimental Data and Results for Integral           271
       Run IR-2-6 (37 - 51 hours)

 4.   Experimental Data and Results for Integral           283
       Run IR-2-6 (51 - 66 hours)

 5.   Experimental Data and Results for Integral           295
       Run IR-2-7 (66 - 81 hours)

 6.   Experimental Data and Results for Integral           307
       Run IR-2-7 (81 - 96 hours)

 7.   Experimental Data and Results for Integral           319
       Run IR-2-7 (96 - 111 hours)

 8.   Experimental Data and Results for Integral           331
       Run IR-2-7 (111 - .126 hours)

 9.   Experimental Data and Results for Integral           343
       Run IR-2-8 (144 - 148 hours)

10.   Experimental Data and Results for Integral           354
       Run IR-2-8 (148 - 156 hours)
                    i
                    i
11.   Experimental Data and Results for Integral           365
       Run IR-2-8 (156 - 168 hours)
                             247

-------
              APPENDIX A-12-1
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-1-4 (188 - 243 hours)
                   248

-------
     S!
                                          -      -              .                                           -  _            2/23/74

                                     STATUS REPORT CF  OPERATING CONCITICNS FC!;.  INTEGRATED OPERATION OF  S02  RECCVERY PROCESS
fO
-P-
:
ij
.1


!;!
4,





OPERATING PERIC3:
DATE: 2/23/74
GATE: 2/24/74





PRCCESS ELAPSED TIKE
P





LES



TIME CF RECCRC: Z3:15 'IRS TC Z4: 0
TIME CF RECCRC: 0: 0 .IRS TC 6:15


CF PERIOD: START 18il.CC HRS / END

HRS
HRS










-
.

243. CO HRS LENGTH CF PERICD: 55.00 HRS
FCR OPERATING PERICO:






->
!*
f'
l".
'"*

••a
n
--
IT


*


3ti
S .
fa"
= s
r.

5 ,
U3
I'-'

>;-
t
>--:

u
5 -'
-..
5

3"
S02 SCR8ER
2:15
6: 15
13:15
17:15
21:15
1: 15
5:15

2:15
6:15
13:15
17:15
2 1 : 1 5
1:15
5:15

23:15
6:15

.
1:15
9:15
17:15
1: 15


2:45
14: 2
3:15
12: 15
l: 2
5:15

19:15
4: 2
11:15
19:15

11:15
19:15
HRS
H.SS
HRS
H.RS
HRS
HSS

HRS
HRS
HRS
H^S
HRS
HRS

HRS
HRS


HRS
HRS
HRS
HRS


HRS.
HSS
HSS
HRS
HR.S"

HRS
HRS
HSS
HRS
HRS
191.00
195. CC
226.00
23C.CO
234. CC
23S.CC
242. CC
A V E

191. CO
195. CO
226.00
23C.OO
234. CO
233. CC
242.00
A V E
188.00
243.00
A V E
19C.OO
195. CO
23C.CO
238. CO
A V c

191.50
2C2.30
216.00
225. CO
237.80
242.00
A V E
134. CO
192.20
2CC.CO
zee. co
316. CO
22''.. t3
Z32.CO
HRS
HRS
HRS
HRS
HRS"
HRS
R A

HRS
HRS
HRS
HRS
HRS
HRS
(ET)
(ET)
ItT)
(ET)
(ET)
(ET)
(ET!
G E_s

(ET)
(ET)
(6T)
(ET)
(ET)
(ET)
H-RS_JLE!J 	
RAGE:
HRS
HRS
R" A
HRS
HRS
HRS
HRS
R A
H.RS
HRS
HRS
HRS
HRS
HSS
R A
HRS
HRS
HSS
HRS
HRS
HAS
(ET)
(ET)
G E :

(ET)
(ET)
(ET)
(ET)
G E :

(ET!
(£T)
IET)
(ET)
(ET)
(ET!
G E :
!ET)
i£T)
SET)
!£T)
(ET!
(ET!
(ET!
S02 CCNC INLET FLUE G->S
S02 CONC INLET FLUE G.'S
S02 CCNC INLET FLUE G"S
S02 CCNC INLET FLUE G/IS
S02 CCNC INLET FLUE G^S
S02 CCNC INLET FLUE G;>S
SC2 CCNC INLET FLUE G-1S
SC2 CCNC INLET FLUE C-,!S

S02 CCNC CUTLET FLUE £S
SC2 CCNC CUTLET FLUE GAS
SC2 CCNC CUTLET FLUE c;*s
S02 CCNC CUTLET FLUE S*S
H20 CCNC INLET FLUE G,!S
H20 CCNC INLET FLUE G..'S
H20 CCNC INLET FLUE G.SS

CRIFICE PRESSURE DRCP
CRIFICE PRESSURE CRCF
CRIFICE PRESSURE DRCP
CRIFICE PRESSURE CRCP
.CRIFICE PRESSURE DRCP

ORIFICE TEMPERATURE
CRIFICE TE'-'PERATtSc
CRIr.ICE TEKFERATLRE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
WEIGHT CYCLCNS CUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNS DUST
HEIGHT CYCLC.\£ CUST
WEIGHT. CYCLCSE OUST
ncIGHT CYCLCN-E CUST
-EIGHT CYClO.E CUST
(GS-
(GS-
(GS-
-
1DP-
10?-
(OP-

(TL-
iTL-
(TL-
!TL-
ITL-
(TL-
(TL-
1 l>~
i 2-
l C-
( C-
( C-
( C-
1 C-
10)
10)
10)
10)
10)
10)
10 )
1C)
16)
16)
16)
16)
16!
16 )
16)
16)
10)
1C)
10)

10)
1C)
10)
10 !
10)

1C)
1C!
10)
10!
1C)
10)
1C!"
11 !
11)
11 )
11 )
il !
U !
11 ;
/ Y10(1,T) =
/ YlO(ltT) =
/ Y1011.T) =
/ YlO(l.T) =
/ YlOi l.T) =
/ YlO(l.T) =
/ YlO(ltT) =
/ AY10A =

/ Y16(1,T) =
/ Y1611tTI =
/ Y16I1.T) «
/ Y16t 1 TT) =
/ Y16(1,T) =
/ Y 16 (l.T) =
/ Y16(1,TI =
/ AY16A =
/ Y10(4,T) =
/ Y10(4,T) «
/ AV10D =

/ C?10(T) =
/ DPiom =
/ CPIC(T) =
/ CP10IT) =
/ AQPIO =

/ TLlOiTj =
/ TLlOiT) =
/ TLIO!") =
/ TLIO(T) <*
1 TLlO(T) =
/ TLIOIT! =
/ ATL10 *
1 C C 1 1 ! T ! =
/ COli(T) »
/ CCll(T) =
/ CD1HT) -
/ CCll(T) -
2C90.000
2296.000
2240.000
2240. COO
2290.000
2290.000
2240.000
2240.857

28.000
70.000
150. COO
175.000
162. ^CO
165. OCC
157.500
131.143
10.000
1C. COO
1C. CCO

2.400
2.400
2.400
2.400
2.400

204.000
308. COO
306. CCO
3C6.COO
309. COO
312. CCO
307. SOO
C.O
1.250
1.200
1.400
1-530
1.6CO
t;
ppy (VCLUKE) .<
PPf (VCLUME) :s
PP." (VCLUME)
PPM (VCLUKE)
PPK (VCLUKE)
P?f (VCLUKE)
PPN (VCLUHE)
PPf ( VCLUME) L-i
_
PPM (VCLUMc) :,
PPM (VCLUKE! M
PPM. (VOLUME) . -,
PPf (VCLUKE! =.
PFH (VCLUHE) '••
PPM (VCLUME) -,
PPM (VCLUME) T.
PPM (VCLUME) .-:
! (VCLUME) b
? ! VCLUME) .;
% 1VCLUME! -^
-_._
INCHES H20 :,
INCHES H20
INCHES H20
INCHES H20
INCHES H20 a
,.
L. tr -j F . i
DHG F
CEG F
CEG f .>
CEG F
CEG F
CEG F
L3 CUST
LS CUST
Lfi CUSI
13 CUST
ie CUST
15 CUST
LB CUST

-------
to
Ul
o
     6
i
1
i
I
(J
1

I
r- 	 ' 	

'••,
^-
, •
;*
[;i
-t
r-

' i
i. ;

11:15 HRS 248. CO HRS
TOT
a a
23: IS HRS 183.00 HRS
<>:15 HRS, 	 - 2ft?. 0.0 HRS
TOT
R A

20:15 HRS 18 5. CO HRS
8:15 HRS 197.00 HRS
TOT
R A

19:15 HRS 184.00 HRS
3:15 HRS 216. CO HRS
11:15 H.?.S 248. CO HSS
A V E S A

6:15 HRS 243.00 HRS
A V E R A


(ET)
A L :
T E :
1ET)
(ET|
A L :
T E :

(ET)
(ET)
A L :
T E :

(ET)
!ET)
(ET)
G E :


LB CUST :.
LB CUST/HR •:
,
LS CUST
L2 CUST
LS CUST
L3 CUST/HR .,
,
? (WEIGHT)
S UEIGHT)
Z [WEIGHT!
t (WEIGHT)

Z (WEIGHT)
? (WEIGHT! ;,
• *
-„
b :»
i* ;*
f*

-------
ro
Ul
      A
t ~ 	
6" 0
L 5:15 HRS 194.00 HRS (ET) *
'! 9:15 HRS 222.00 HSS ?ET) S
si 9:15 HRS 246. CO HRS (ET) %
• '• AVERAGE:?
i.;
•il 5:15 HRS 194. CO HRS (ET! S
!•: 9:15 HRS 222.00 HRS (ET) X
!•' 9:15 HRS 246. CO HRS (ET) %
•! AVERAGE:?
I A
TOT
TOT
TOT
TOT

H20
H20
H20
H20
>• 23:15 HRS 138.00 HRS SET) WEIGHT
;<•: 6:15 HRS 243. CO HRS (ET! WEIGHT
;: TOTAL: WEIGHT
;> R A T E : Wr
i.1
'••i 6:15 HRS 243. CO HRS ( ET ) S
» AVERAGE:?
IGHT
TOT
TOT
CARBON PR
S ON INLET CAFEH,
S CN INLET CAFEC1,
S CN INLET CAf ECK

ON INLET
CN INLET
CN INLET
CN INLET
CYCLCNE
"CYCLCNE"
CYCLCNE

CARBCfv
CARETS
CARBON
CARBCN
CL'ST
DLST
DUST
CYCLCNE DLST
S CN CYCLONE LLST
S CN CYCLCNE TLST
E C 0 N 0 I
5CS-301)
(CS-30U
ICS-301)

JCS-3C1 )
(CS-301 )
l f c "i r. i 1
«CS-3C1)
C-301)
D-301 i
D-3CI)
D-3C1 !
D-301!
0-301 )
T
/
/
/
/

/
/
/
/
/
/
/
/
I 0 N E R
Z30K1.T) =

Z3CI!1,T) =
AZ301A =

Z30H2.T) =
Z30K2.T) =
Z301I2.T) =
AZ301B =
CD301IT! =
CD301 (T) =
W3301 =
R2301 =
D30K1.T) -
AD301A «
8
8
8
8

5
5
9
6
0
0
0
0
0
c
2/23/74 PAGE 3 ^
1
.880 * (WEIGHT) j
.540 ? (WEIGHT) :-"!
.COO S (/.EIGHT) ;;
.480 3 (V(EIGHT) ;>
.050
.870
.330
.750
.0
.0
.0
.0
.0
.0
1.
1 (WEIGHT) \.\
1 (WEIGHT) ;.:
% (WEIGHT) '-
! (WEIGHT)
LB CUST -.
LS CUST
LB CiJST .;
L8 CSJST/HR ^
3 (WEIGHT) :-,
? (WEIGHT) -,'

"•• r
2: ' -~>
** -j
?> XJ


_J








--
»i - •" J
=•»•'

















-,
3,'
F; .
        £r

-------
      '-y
ro
Ul
i
f'i
,«!


iv
F*
20:26 HRS
0:
17:
23:
4:
17:
22:
6:

15
15
32
32
38

HRS
HRS
HRS
HP.S

233
237
t.
2C5
212
217
23C
235
243
A
.20
.CO
V z
.90
.CO
.30
.30
.40
V E
HRS
R A
HRS
HRS
HRS'
HRS
K«S
R i
(ET)
1ST)
G E :
IET)
(ET)
(ET)
(ET)
(ET)
(ET)
G £ :
S02
SC2
SC2
H2S
H2S
H2S
H2S
H2S
H2S
H2S
CONC
CCNC
CC^C
CCNC
CCNC
"CONC
CONC
CCNC
CCNC
CCNC
SULFUR
CUTLET GAS
CUTLET GAS
CUTLET CAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
:NLET GAS
INLET GAS







t. •
b
;j
L1
•-
rz
f
C'

fc*
2«.
C*
P

: i
S3
3*
bs
?•
!j 	
^
-.
•^
P
.
(t-
•jj
'"
„
A2
,_
•-
20:
0:
17:
23:
4:
17:
22:
5:


16:
2C:
0:

23:
4:
17:
22:
6:


26
15
8
15
32
32
38
26
32 ~
26

jg
32
32
33
26


20:26
0:
17:
23:
4:
17:
22:
6:


20-.
0:
2:
21:
9:
17:
5:
15
8..
32
32
38
26
15
15
H
HP.S
HP.S
HRS
HRS
HRS
HRS
HRS


HRS
HRS
HRS

HRS
HRS
HRS

T'RS
HRS
HRS
HRS
HRS
HRS
HRS

HRS
HRS
HRS
HRS
hSS
HRS
233
237
A
2C5
212
217
.20
.CO
V E
.90
.CO
. 30
23C.30
235.40
243.20
A

229
233
237
A

212
217
V..E.
.30
.20
.CO
Y...E.
.00
.30
23C.3C
235.40
243. 20
A V E_

233
237
A
2C5
212
217

.20
.CO
V E
.90
.CO
. 30
23C.30
235.40
243.20
£

233
237
A
191
21C
222
23C
242
v e
.20
.00
V E
.CO
.00
.CO
.CO
.CO
HP.S
HP.S"
R A
HRS
HRS
HRS
HRS
HRS
HRS
R A

HRS
HP.S
HRS
R A

HRS
HRS
HRS
HRS
HRS
R A

HRS
HRS
R A
HRS
HRS
HRS
HRS
HRS
±?s.
Q A
HRS
HRS
R A
HRS
J-RS.
H.^S"
i-RS
(ET)
(ET)
G £ :
(ET)
(ET)
IET)
(ET)
IET)
!ET)
G E :

(ET)
(ET)
(ET)
G E :

(ET)
iET)
!ET)
(ET)
(ET)
G E :

(ET)
(ET)
G E :
(ET)
(ET)
(ET)
IET)
(ET)
(ET)
G E :

(ET)
(ET)
G E :
(ET)
(ET)
[ET)
! ETi
(ET)
H2S
H2S
H2S
H2
H2
H2
H2
' H2
H2

H2
H2
H.2
H2

CCNC
CCNC
CCNC
CCNC
CCNC
CCNC
CCNC
CONC
CCNC
CCNC..
CCNC
CCNC
CCNC
CONC

	 H20 CONC
H20 CCNC
H.2C
H20
H20
H20

H20
H20
H20
N2
N2
N2
N2
N2
>\2
N2

N2
N2
N2
N2
N'2
N2
\ 2
N2
CCNC
CCNC
CCNC
CCNC

CCNC
CCNC
CCNC
CGNC
CGNC
CCNC
CQNC
CCNC
CC.NC
CONC...
CCNC
CCNC
CCNC
INLET
INLET
INLET
IM.2T
INL6T
CUTLET GAS
CUTLET GAS
CUTLET GA3
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS

CUTLET GAS
CUTLET GAS
CUTLET GAS
CUTLET GAS

INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS

CUTLET GAS
CUTLET GAS
CUTLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET GAS
INLET CAS

CUTLET GAS
CUTLET GAS
CUTLET GAS
VCL FLC'n R
VCL PLOW ».
VCL FLC* *
VCL rLCW R.
VCL FLCi> *
—





—

—














.17:
ST
17
IT:
GENERATC
(GS-2C6)
(GS-2C6)
(GS-206)

31
=3
ra
(GS-206)
(GS-206)
{GS-2C6)
(GS-206)
/ Y2C6(3,T) =
/ Y206!3rT ) =
/ Y20613.T) =
/ AY206C =
0.0
0.0
0.400
0.133
% (VCLUME) .
* (VCLUME)
? (VCLUME)
S (VCLUKE)
-t
r*
r«
(GS-200)
(GS-2CO)
(CS-2CC)
(GS-2CC)
(GS-200)
(GS-2GO)
/ Y200I4.T) =
/ Y200(4,T) =
/ Y2CCi4,T) =
/ Y200(4,T) -
/ Y200(4,T) =
/ AY2000 =
1K400
11.8-00
10.200
12.800
14.600
12.160
S (VCLUME)
S (VCLUME)
S (VCLUKE)
? (VCLUME)
? (VCLUMEI
S (VCLUKE)
..
^
:2
Z3
^
;«
(GS-206)
- (GS-2C6)
! GS-206)
(GS-2CC)
(GS-2CC )
(GS-2CO)
(GS-2CO)
5GS-20C)
(GS-2CC)
• (GS-2CO)
/ Y2C6(4,I) -
/ Y206i4,Tl =
/ AY206C =
/ Y200(5,T) «
/ Y2CO!5tT) =
/ Y2CC(5tT) =
/ Y2CC!5,T! =
/ Y2CO(5,T) =
/ Y2CC(5,T! =
/ AY200E =
48.900
47.600
57.700
55.600
55.200
~ 56.700
55.300
54.2CC
55.7S3
S (VCLUME)
S (VCLUME)
S (VCLUME)
S (VCLUME)
? (VCLUME)
% (VCLUME)
* (VCLUME)
? (VCLUME!
S SVCLUME!
-^
~.
-O
JT'
-:
.1
»•>
_.
(GS-2C6)
(GS-206)
(GS-206)
I G-2CC!
( G-2CC)
( G-2CC)
I G-2CO)
( G-2CO)
/ Y206(5,T) =
/ Y206!5,T) =
/ AY206E =
/ G2C3!5,T) =
/ G2QC(5,T) «
/ G200(5t7) =
/ G2CO!S,T) =
47.500
49.900
48.700
150.000
150. COO
150. COO
1 > 0 . 0 C G
150. 'COO
% (VCLUME)
S (VCLUME)
% (VCLUMEI
CFH (70 CEG F)
CFH i7C EEC F)
CFH !7C CcG Fi
CFH !7C D=G F)
CFH <7C CEG F)
*t
rf»
a
.,
-7
^
-\

-------
N>
Ui
U>
                                   AVERAGE:
                                                       N2 INLET VCL FLOW RATE
                                                                                       <  G-2CC)  /
                                                                                                     AG200E
                                                                                                                       2/23/74      PAGE   5

                                                                                                                  150.000 CFK  (70  CEG F)
^


III
; I
•7.
fte

K
P
fV
':>•
IT
5:15
9:15
9:15

9:15
HRS
HRS
HRS

HRS
9:15 HRS
5:15
9: 15
9:15

5:15
9:15
9:15

HRS
HRS
HRS

HRS
HRS

194. CO
222. CC
246. CO
A V £

222.00
246.00
A V E
194. CO
222. CO
246.00
A V E
1S4.CO
222. CO
246. CO
A V E
HRS
HSS
HRS
R A

HRS
HRS
R A
HRS
"HRS
HRS
R A
HRS
HKS
HRS
R A
(ET)
(ET)

-------
Ul
r
;
ji

!
t;
I
t
•1
IT!
1— —
>' - -
j
!"r
;••
K
P
M
i»
r.
W
pr
!»'
23
?: fl
21:15
17:12
7 7- •3d
6:26
...2= 8
21:15


17:32
22:38
6:26

17:32
22:38
6:26

17:32
22:38
6:26
2:15
21:15
9:15
2:15
5: 15
HRS
HRS
HRS
LiO C
HRS
HRS
HRS


HRS
HRS
HRS
	 	
HRS
HRS
HRS

HRS
HRS
HRS
_H_S_S 	
HRS
HRS
HRS
HRS
19C.90 HRS
234. CO HRS
A V = R A
23C.30 HRS
3 2 e * n uo e
243.20 HSS
19C.VO HSS
234. GO H^.S
A V £ R A

23C. 30 HRS
235.40 H=S
243.20 HRS
AU "" O f

23C.30 HRS
235.40 HRS
243.20 HSS
A V E R A

23C.30 HRS
235.40 HRS
2^.2.20 1-RS
A V E R i
H 2
(ET)
(ET 1
G E :
(ET)
1 CT 1
(ET)
(ET)
(ET)
G E :

(ET)
(ET)
(ET)
Ge •

(ET)
(ET)
(ET)
G E :

(ET)
(ET)
(ET)
G E :
191. CO HRS (ET)
21C.CC HRS
22Z.CO HRS
23. CO HSS
242. CO HRS
A V E R A
(ET)
IET)
(ET)
(ET)
G E :
S GENERATOF/SU
H2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H,2 CONC CUTLET GAS
H2 CONC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CONC CUTLET GAS
N2 CCNC INLET GAS
N2 CONC INLET GAS
N2 CCNC INLET GAS

N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
*•' "> f*H R i" PI'Tl CT f" A C

H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H.2S CONC CUTLET GAS

H2Q CCN'C CUTLET GAS
H2C CCNC CUTLET GAS
H20 CCNC CUTLET GiS
H20 CCNC CUTLET GAS
• N2 INLET VCL FLOW RA"E:
N2 INLET VCL FLCh RATE-
N2 INLET VCL FLCV< RAT?
N2 INLET VCL FLCK RA~£
N2 INLET VCL FLCK RA7E:
N2 INLET VCL FLOW RATE
L F U R S
(GS-1CC)
(GS-1CCI
(GS-1CC)
(GS-108)
(GS-1CE )
IGS-lCt)
(GS-ICS)
5GS-1CC)
(GS-1CC)
IGS-1CC)

(GS-ICB!
(Gs-icei
SGS-ICE)
( G5-1C S i
IGS-106)
(GS-lOc)
(GS-lCc)
JGS-1CS!

IGS-108)
(GS-1C6)
(GS-ICo)
 	
(ETI
IET)
(ET)
A L :
T E :

!ET!
(~T)
A L :
T E :

(ET)
(ET)
G £ :
:ETJ
G E :
HEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DLST

WEIGHT FILTER CUST
ViEIGHT FILTER CUST
WEIGHT FILTER CUST
WEIGHT FILTER CUST

3 TOT S CN CYCLCNE C";ST
* TOT S CN CYCLCNE 0:,ST
S TOT S CN CYCLCNE C'J-ST
% TCT S CN FILTHS D'J H
y TOT S CN FILTER O'J'ST
0-101)
C-1C1)
D-1C1 )
D-101)
( D-101)
{ D-101)

{ D-102)
( D-102)
t D-1C2)
( D-102!

1 D-1CIJ
( 0-101)
J D-ICi)
( D-1C2)
< C-1C2)
/ CD10KT)
/ CD10KT)
/ C010KT)
/ CD10KT)
/ V.'D1C1
/ RD1C1

/ CD1C2(T)
/ CC102!T)
/ W31C2
/ R0102

/ 010K1.T)
/ ElOUl.T)
/ AD101A
/ C102(1,T)
/ A0102A
=
=
ss
=:
=

=
=


=

=
0.0
0.176
0.322
0.263
0.761
0.014

0.0
0.0
0.0
0.0

31.600
30.700
31.150
0.0
0.0
LB CUST
LB CUST
LB CUST
LE CUST
L8 CUST
LB CUST/HR

L2 CUST
L2 CUST
LB CUST
LB CUST/HR

3 (WEIGHT)
S (HEIGHT)
?' UEIGHT)
% (V.EIGHT)
% (WEIGHT)
15
••*!
H
•^
^,
'•4
}
-«
j
^
•i
!.-!

-------

; •


!
i
>•
*
T!
;1
i«J
iX
ii
j>
r-
n
3J
10 :J
Ol Is!
LJ
i -

u
?•;
5:15 HRS 194.00 HRS (ET)
9:13 hRS 222.00 HRS (ET)
9:15 HRS 246.00 HRS (ET)
AVERAGE:

5:15 HRS 194. CO HRS (ET)
9:15 HRS 246. CC HRS (ET)
AVERAGE:
23:15 HRS 188. CO HRS (ET)
9:15 H*S 246.00 HRS (ET)
AVERAGE:


23:15 HRS 236.00 HRS (ET)
5:15 hRS 242. CO HRS 
RATE
RATE
RATE

FUR C C t
CCLLECTE;
COLLECTS:
CCLLECTES
CCLLECTEC
CCLLECTEC








iCS- 9C) /
(CS- 90 /
ICS- 9C) /

(CS- 90) /

y
!,
M
i;
S
!"
I,
H
f>
b*
H

£<
ij
a
	 	 j
-T
y
*
•' i
t
u

-------
                                                                                                                      2/23/7*

                                    STATUS REPORT CF OPERATING CONDITIONS FCR INTEGRATED OPERATION OF S02  RECCVERV  PROCESS
                                                                                                                                  PAGE
NJ
Ul

j;
.•
•





OPERATING PERIOD:
	 QiT = : 2/23/74 T1XE CF RECCRC

PROCESS ELAPSED TIME CF PER.ICO:


0: C rK
START 168..
": sitMKARY CF INTEGRATED PROCESS PERFORMANCE:
S
.:-
b
r *
r*
("•'
i«
.V

1.

2.
3.

4.

S02 REMOVAL

H2S UTILIZATION
ACIO CONVERSION (TO SULF'JR)

1-2 UTILIZATION (TO H2S)

PRS02 =

PVCS *

PHCHS =
j
S TC 24: C HRS
I C 6s 1 5 rRS i
CC HRS / ENC 243.00 f-RS LENGTH OF PERICC: 55.00 HRS v
-— — — •- 	 	 • 	 • 	 •-• 	 i
T
, i
9
94.15 Z (ACTUAL) 90. C S (GCALI ,-t
'.,
9C.97 S (ACTUAL) 95. C J (GOAL) ;«
•4
36.56 % (ACTUAL! 99.0 J (GOAL) W
rJ
72.29 % (ACTUAL) 90. C I (GOAL) - >J
r» §'
-
y
5.
6.
SULFUR RECOVERY
H2 UTILIZATION 4" UNIT
PRS
PUH2 =
63.38 % (ACTUAL) 1CO.O 1 (GOAL) OF SCRBEC SC2
18.34 Z (ACTUAL) 25. C S (GOAL) OF STRIPPED SL'LFUR a
93.53 % .-,
=» 71
i*:
"•*;
r.
••*
w
K
T;
i ;
7.
8.
5.

1C.
11.
RESIDUAL SULFUR ON CiRECN
CARBON RECYCLE RATE IDS)
ACIO LOADING INLET CAREON 6" UNIT

MOISTURE CCNTENT INLET CARBON 6" UNIT
ACID LOADING INLET CiRECN 8" UNIT
^ i?. nnrsTURF CCNTENT INLET CARBCN 8" UNIT
:i
3*
r"
U


"i
w
HI.
,
13.
14.

TOTAL AC'D CONVERTED 6" UNIT
SULFUR CONVERSION (TO K2S)
L">T Sill PLR TPNCENSER EFFICIENCY




X9CA =
RC90 =
X301C -

X301B »
X302C =
X302B =

PVC
PSCI-S =
ERV400=


fAJCR EVENTS CURING OPERATING PERICC:
SCIVED PRCBLEC ViITH OFF-GAS ANALYSIS FROM SUl

AT ENC CF PERICC LOWERED hYCRCGEN
C.C337 L8 S/L6 C w
29.922 LB C(DB)/HR . " jj
:J
C.256C LB ACIC/L8 C -:
^
C.C934 L8 H20/LB C s»
, !
C.256C LB ACIC/LB C rf
C.0934 LB H2C/LB C ^

?5.59 * • ^
87.40 S p
1*5.58 S a
''•

U
FJR GENERATOR J
FLOW RATH TO 120 CFH

-------
N)







STATUS RP.PCRT CF OPERATING CCNCtTICNS
OPERATING PSRIOC:
DATE: 2/23/74 TIME CF RECCRC: 23:
CATE: 2/26/74 TIME OF RECCRC: 0:

PRCCESS ELAPSED TIXE CF PERIOD: START
SULFUR MATERIAL BALANCE (USING PRCCESS H2S):

FCR INTEGRATED CPERATICN
IE t-RS TC
0 HRS TC

188. CO HRS


24: C
6: 15
~7~ENO


HRS
HRS

243. CO


2/23/74
CF S02 RECCVERY PROCESS



HRS











LENGTH OF PERIOD: 5


PAGE 9 ")
\
J

',.
:
S:00 HftS !.
1
' 1
..

p


;
r
E


tt
r
S 0 2
; N
INLET GAS AS S02
INLET C AS RESIDUAL S
TOTAL IN:

CUT
OUTLET GAS AS S02
CUTLET CARSON
CYCLCNE CUST
CCLLECTCR DUST
CiRECN WEEPAGE
TCTAL OUT:
6" DIA CARBO
s c: R B
( ',- l!i> I
( C- lit 1
t S i- 1 (i ) /

( c- i;:) /
( :> li.) /
< ':- i;:> /
(C'.- K'l /
 /
R GEN

BC12A
SI300

BC201A
BD301A
S0300
ERA


3.5C93
3. 5093

3.
C.
3.
T C R

5093
0
'5C9~3


LS
LS

LB
LB
LB


SULFUS/HR
SU'LFUR/HR

SULFUR/HR
SULFUR/HR
S'JLrUR/HR

^
-'
-^
'.i
:.,
r.-.
^1
t1' '«.'
«;
ft!
Ai/
,7"
»S
•I?1
K;
t N
INLET GAS AS H2S tCYL)
INLET GAS AS H2S (PRCC)
INLET CARBCN
TCTAL IN:

CUT
CUTLET GAS AS H2S
OUTLET GAS AS SC2
OUTLET CARBON

{ c-zc;.) /
< C-iCi ) /
t c-jc:. > /

-------
NJ
Ul
CO

1' *
i';
3]
'4,
•V
'*•
1
* '•

r*
i?
»i
''i.

H 2 S
GENERATOR
I N
INLET CARECN


CUT
CUTLET
CLTL3T
CUTLET
CYCLCNE
FILTER
T

T C T


CA°.3CS
GAS AS
GAS AS
CUST
CUST
C T A
C
A L IN:

'
H2S
S


L CUT:
V E R A L L
( C-
1RV-


( C-
< G-
( C-
( 0-
(RV-
S L L
•'SULFUR
•C2)
'.CO


!.C3)
:.c^t)
id)
1C2)
:.cc>
F U
/ 3C202A
/ SHOO


/ SC103A
/ BG1048
/ SCIONS
/ BD101A
/ 8D102A
/ S0100
R 8 A
S T
=
_


C
•s
-
S
9
9


1
7
1
C
0
R I P
.7849
.7849


.OC85
.6705
. 6 i C C
-C042
.0
= 10.2933
t A
N C
E
P E
L8
LE

L3
LE
LE
LS
LB
LS

2/23/74 PAGE 10
R
SULFUR/HR !>
SULFUR/HR i.
'Si
«.
SULFU'S/HR '•;
SULFU3/HR ;,
SULFUR/HR iJ
SULFUR/HR I,,1
SULFUR/H.R Ijj
j
rfa f h
--
I N

-i INLET GAS 18"
t :
•X
:r
-t
INLET G
CUT
CUTLET
CYCLCNE
AS 8"

GAS 18
CUST

UNIT AS SC2
UNIT AS CYL H2S
T C T A L

" UNIT AS SC2
13" UNIT
-.;. CCLLECTC3 DUST IS" UMT
=> CASECV XEErAGE 13" UMT
~ CYCLCNE CUST 6" UNIT
cv
•~.
'x
??
S*
21
OUTLET
•OUTLET
CUTLET
OUTLET
CYCLCN;
FILTER

«
GAS 8"
GAS 8"
GAS 4"
GA S 4 "
CUST
CUST 4


UNIT AS H2S.
UNIT AS SC2
UNIT AS H2S
UNIT AS S
4" UN: IT
" UNIT
TOTAL S


t 3-
S L t

I G-
( C-
( C-
(CV.-
( C-
( G-
( G-
( G-

1C)
F U

13)
Hf
121
i.21
,!C5)
:;c5 )
1C4 )
{ C-iOl!
! C-IC2)
U L P

U R


/ BG10A
/ BG201B
R I N

/ 8G13A
/ BDUA
/ S012A
/ BCK12A
/ EC 301 A
/ BG2Q58
/ BG2D5A
/ seiche
/ 8G104S
/ ED 101 A
/ HC102A
OUT


X.
•

=
=
=
;=
=
=
=
=
:


2
C
2

C
0
f*
c
0
0
0
c
1
0
2


.6933
.0
.6983

.1579
.~G170"
. CO 1 2
.0
.6331
.2359"
.C
.6100
.00<.2
.7253


IB
LE
LB
LS"
LE
L S"
IB
LB
LB
LS
LS
» P
LS
LB

','
SULFUR/HR '^
SULFUR/HR i,
SULFUR/r.R - . ''ri
...
SULFUR/HR 7i
SULFUR/HR T<
SULFUR/HR aj
SULFUR/HR " W
SULFUR/H3 V
SULFUR/HR :i
SULrUR/HS . -j
SULFUR/HR „'
SL'LF^R/HR ,.
SliLFUR/i-S :-
SULFUR/HR ^
B?
3* 3«(

^










































1
^i

,.
j*
», •**
"5
«;

       rt-

-------
                                                                                            2/23/74
                                                                                                        PAGE 11
hVCRCGEN MATERIAL  BALANCE:
t[
I*
•',.
'L

! N


S U L F

INLET GAS AS H2
•i_ INLET GAS AS H2S (CYL)
f .
i
*.-
•»
INLET GAS AS H2S (PRCC)
INLET GAS AS 1-20
INLET Ci'KSCN


T C

T A L IN:

UR GENERATC

! G-rC3) /
{ 6-ZC3> /

' BG203C =
' BG203B =
1 G-l':3) / EG203 =
( G-rOS! / BG203D =
( c-?/:i) / ec2o\ir =
(RV-::CO /

' H20C =

R

0.
c.
c.
c.
0.
1.



C09/
0 "
4793
1663
4S67
1420


LB
"LB"
LS"
Le
LE
LE


HYCRC-GEN/f-R
HYCRCGEN/hR
HY:RCG=N/HR
HYCRC5E.M/HR

'='
.
:
.;
>
9
•
CUT

:i
,j
•5
:--.
-.:
ts_"i "^
in -*-
VQ '"'
W
*»
!*
;-i
OUTLET
OUTLET
CUTLET
CUTLET
T


I N
INLET
I'iLET
CUT
OUTLET
CUTLET
CUTLET
T
GAS
GAS
GAS
AS H2
AS H2S
AS H2C
CAR3CN
C T

H 2

GAS
A L CUT:

S GENERA

AS HZ
CAR3CN
T C
GAS
GAS
GAS
C T
T A U IN:
AS 1-2
AS (-2S
AS h20
A .L CUT:
{ G-:.:-:5> /
( G-::I:SJ i
f G-.1 :s ) i
\ C-2C2) /
!RV--1CC) 1

T C R / 3 U

1 G-l'3) >
! c-?:: ) >
(Rv-t:ci /
i • G-I:«) /
{ G-i;^) /

IRV-ICC) y
' BG2C5C =
' EG205H =
' EG205C =
' SC2C2r =
' 1-C20C =

L F Li R

' BG103C =
' BC202H =
' HI IOC =
' BG104C =
' BG104H =
' BG104D =
' i-OiOO =
0.
r\ ^
C •
^
U •
0.

S T R

C.
C.
C.
0.
0.
r>
•* *
0.
0023
C43C
O 7 c £
0 2 19
9025
I P
6630
0219
6C49
0093
4 793
1934
6624
LB
LE
LB
i- £?

P E

LE
LE
LE
L8
"LE"
LE
LE
HYCRCGcN/HR
HYCRCGEN/HR
hYCRCGEN/r-R
HYCRCGEN/I-R

R

HYCSCGEN/hR
HYCRCGS^/t-R
HYCRCGEN/KR
HYCRCGEN/hR
HYCRCGEN/hR'
HYERCGEM/VR
HYCRCGEM/rR
&
>
-
•a
^
T;
~3
-t.
.
--•
;,
-,
JO
-
i*1 ' K
?J



















• i
*

-------
              APPENDIX A-12-2
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-1-5 (246 - 262 hours)
                   260

-------
                                                                                                                     2/26/73
                                                                                                                                 PAGE   1
Ni
                                   STATUS REPORT CF OPERATING CONDITIONS FOR INTEGRATED OPERATION CF soz RECOVERY PROCESS
(:>. 	
i.-i
i.i


V
v
i''

OPERATING PEPICO:
CftTE: 2/26/73 TIKE OF RECCRC: "• 9:15 h>< TC 24: 0
CATE: 2/27/73 TIME OF RECCRC: 0: 0 h-.S TC 9:15


PROCESS ELAPSEC TIPE


CF PERICD: START 246 .CO HRS / END
HRS
HRS

270.



: 't
i'!
,,l
CO HRS LENGTH GF PERIOD: 24.00 HRS :.l
PROCESS VARIABLES FCR OPERATING PERICD:






h
i
~y.
'•«• ^
>r
is
M
'•r
.i*

72
=3
•"•I
"""•

W
~i
\"
r*


'•
j.

1 ^

r"

'4i
r '

'.^
•^


13:15 HRS
18: 2 HRS
21:15 HR S
l: 15 H.RS
5:15 HRS
13:15 HRS
19: 2 HRS
21:15 HRS
1:15 HRS
5:15 H.RS
21:15 HRS


13:15 HRS
22:15 HSS
6:15 rRS


13:15 HRS
22:15 HRS
6:15 HRS

11:15 V-RS
3:15 HRS

11:15 HRS
3: 15 HRS

16:15 HRS
0:15 H.RS




25C.OO HRS (ET)
254. SD HRS (ST)
25c.CC r 3 S ( C T )
262. CO HRS (ET)
266.00 H?.S 
267. CO j-'S (ET!
AVERAGE:

243. CO HRS (£T)
254.00 H=.S (ET)
T C T A L :
S i T E :
243. :C r?S (ET)
264. CD !--. S IcT)
T G T 4 L :
RATE:
253. CO HRS (ET)
261.00 HRS (ET)
TOTAL:
5. - T E :

S 0 2 3 C R
S02 CCNC INLET FLLE G*3
S02 CCN'C INLET FLUE G/3
S02 CGNC IN-Lci FLUc Gti
S02 CCNC I.NLET FLLE GAS
S02 CCNC INLET FLUE G«S
S32 CCNC INLET FLUE G«S
S02 CCfiC CUTLET FLUE G4S
S02 CCNC CUTLET FLUE G«<
S02 CONC CUTLET FLUE G££
S02 CCNC CUTLET FLUE GAS
S02 CCNC CUTLET FLLE G*£
S02 CCNC CUTLET FLUE Gi£
H20 CCNC INLET FLUE G/S
H20 CCNC I.NLET FLUE G-
1CX-
(Ci*-


10) /
10) /
1C ! /
10) /
1C 1 /
10) /
16) /
16) /
16 ) /
16) /
16! /
10) /
10) /

1C! /
10) /
10) /
1C) /

1C ) /
1C! /
10 ; /
1C ) /'
IT * /
L t 1
11) /
11 !/
11! /
12 ) /
12) /
12 ) /
12) /
12! /
12) /
_-2.l./.

Y 10 ( 1 T T ) =
Y10(1,T) =
10 ( 1 » T ) —
YlO(ltT) =
YlOIltT) =
AY10A =
Y16!1,T) =
Y16!1,T) =
Y16U,T) =
Y16! 1 f T ) =
Y16(1,T) =
Y 1 0 ! 4 1 T i =
AY10C =

CPiOIT) =
C? 10 IT) =
DPIO'.T) =
SOP10 =

TL10(T! =
TLlO'Ti =
TLIC;T) =
A 7 L 1 C =

COU(T) =
CC11 IT! =
^D! 1 =
CC121T) =
C012!T) =
K012 =
RD12 »
CVJ12 (T ! =
V.'C'
9. £00 S (VCLU'ME) t=
9.SOO S iVCLUri = ) ~:
-,-•
2.400 INCHES H20 •..;
2.400 INCHES H20 ..
2.250 INCHES H20 ;,:
2.383 INCHES H20 -j
ES
2C7.000 CFG c r.
30?,. COO CSG r
203. COC CHC F
2C4.333 CEG F ;,
,
0.0 LE CUST ;
4.200 L? C'JST
4.2".'0 LE COST
o..c£2 Lr :JST/HR
-1
C.O Li CUST
2.700 L= CUST ' .,
2.700 is :usr • ' ' ,
0.169 IB CUSI /HR •
C.O Lc CUST ,:
O.C54 LZ CUST ,,
O.C56 LE CUST .]
O.COV LS CUST/HR
;,
                       11:15 HRS   2-3.CO HRS iET)
                                                       S TGT S  CN  CYCLCNE  2LST
                                                                                       C- II) / C1K1.T)  =
                                                                                                                  7.0feO ?  (HEIGHT)

-------
N>
          AVERAGE  :

._5_HAS	C._0 2_N R S_l £ Tl

          A V ~E R A G E  :
                                                          S  TOT S CN CYCLCiNE

                                                         _?_TPLJL_CN_CC|-LECTQR_ CI S L
                                                          x  TOT s CN cciVecTOR "ci.sr
<  D- 11) /

I  D- 12) / C12U.T)
   2/2f/73      PAGE   2

7.0cO t  (WEIGHT)

7.060 X  (HEIGHT)
                                                                                          < D- 12) /
                                                                                                        A012*   =
                             _
                              7. "080
                                                                                                                                U EIGHT)

-------
to
i
I 6" 0 I A
v 17:15 HRS 254.00 HRS ( ET ) ? TOT
pi 1:15 HRS 262. CO HRS (ET) S TOT
i'j 5:15 HRS 266.00 HRS (ET) % TOT
|'L_ • AVERAGE:* TOT
'•*!
!'i 17:15 HRS 254. CO HRS (ET) % H20
•: 1:15 HS.S 262. CO HP.S 1ET) 1 H20
iri 5:15 HRS 266. CC HRS (ET) t H2C
!«! AVERAGE:? H20
f» 9:15 HRS 246.00 HRS (ET ) WElGt-T
'•> 9:15 HRS 27C.CO HRS ( ET ) WEIGHT
«! TOTAL: WEIGHT
»i RATE: V.EIGHT
U: 9:15 HRS 27C.OO HRS tET) S TOT
}*' . A V E R A G E : % TOT
•!«
-«
t".
C7
&
u
C A R 8 O. K PR
S ON I\'LET CAR8CN
S CN INLET CAPSCN
S CN INLET CAPECN
S CN INLET CAHeCiV

CN INLET CARBCN
CN INLET CARBCN
CN INLET CARECN
ON INLET CAR8CN
CYCLCNE OUST
CYCLCNE OUST
CYCLCNE OLST
CYCLCNc CUST
S CN CYCLCNE DUST
S CN CYCLONE CLST






E C 0 N C I
•CS-301 )
(CS-3C1)
fCS-301 1
(CS-301)

(CS-301)
(CS-301 )
(CS-301)
(CS-301 )
( 0-301)
( 0-301)
« D-3C1)
{ D-301)
( 0-301)
( 0-301)






T
/
/
/
/
"/
/
r
/
i
/
/
i
i
i






t 0 N c R
Z301U.T) =
Z30K1.T) =
Z3GHltT) =
AZ301A = .

Z301I2tT) =
Z30K2.T) =
7 3O 1 I ? . T 1 ~
AZ301B =
C030KT) -
CD30KT) =
WD301 =
RD301 =
0301(1. T) =
A0301A =






2/26/73 PAGE 3
8.440 t (V.EIGHT)
7.600 * (WEIGHT)
8.560 ? (WEIGHT)
8.200 * ( HEIGHT)

7.790 3 (HEIGHT)
7.460 3 (ViEIGKT)
6.790 % (V,EIGHT)
7.347 S (hEIGHT)
0.0 LB CUST
0.0 LB CUST
0.0 L3 CUST
0.0 L3 CUST/HR
0.0 S (WEIGHT)
0.0 S (KEIGrT)


•-





'.
:
t
,';
--.

7J
,'4
r*
-*
...
-i
»
-2
13
-*
H '
fc! -.
1 :
f> '•>
P




-
13
HI
pi
(-(-._.
P
C-
	
I-!
Ij 	 	 "








,


























-,
-,

_;
t.
•— • • i '
-i

-------
                                                                                                                         2/26/73
                                                                                                                                     PAGE
to
                                                                 SULFUR
                                                                                 GENERATOR
1,4:45 HRS
23: 2 HRS
12:32 HRS
0:15 HRS

i 14:45 HRS
E

12:32 HRS
' 0:15 HRS
i
n
I 14:45 HRS
23:26 HRS
i
12-32 HRS
: 0:15 HRS


14:45 HRS
i 23:26 HRS
'
12:32 HRS
0:15 HRS
•
14:45 HRS
23:26 HRS


9:15 HRS
9:15 HRS
21: 15 HRS


21:15 HRS
21:15 HRS


21: 15 HRS
9:15 HRS
17! 15 HRS
1:15 HRS
5:15 HRS
251.50 HRS (ET)
259.80 HRS (ET)
AVERAGE :
249.30 HRS (ET)
261. CO HRS iET)
AVERAGE:
251.50 HRS (ET)
6C.20 HRS (ET)
AVERAGE:

249.30 HRS ( ET )
261.00 hRS (ET)
AVERAGE :
251.50 HRS (ET)
26C.20 HRS (ET)
AVERAGE:
249.30 HRS (ET)
261. CO HRS (ET)
AVERAGE:

251.50 HRS (ET)
26C.20 HRS (ET)
AVERAGE :
249.30 HRS ( ET )
261. CO HRS (ET)
AVERAGE:
251.50 HRS (ET)
26C.20 HRS (ET)
AVERAGE:

246.00 HRS (ET)
27C.CO HRS (ET)
AVERAGE:
253. CO HRS (ET)
AVERAGE:

253.00 HRS tET)
AVERAGE:
258.00 HRS !ET)
AVERAGE:

258.00 HRS (£T)
AVERAGE:
246.00 HRS (ET)
254.00 HRS (ET)
262. CO H?S IcT) 	
266. CO HRS i£T)
AVERAGE :
S02 CONC CUTLET GAS
SC2 CONC CUTLET GAS
S02 CCNC CUTLET GAS
H2S CONC INLET GAS
H2S CONC .INLET GAS
H2S CONC INLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CGNC CUTLET GAS

H2 CONC INLET GAS
H2 CONC INLET CAS
H2 CONC INLET GAS
H2 CCNC CUTLET GAS
H2 CON'C CUTLET GAS
H2 CCNC CUTLET GAS
H2C CCNC INLET GAS
H20 CCNC INLET GAS
H20 CONC INLET GAS

H20 CCNC CUTLET GAS
H2C CONC CUTLET GAS
H20 CCNC CUTLET GAS
N2 CQNC INLET GAS -
N2 CONC INLET GAS
N2 CONC INLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
M2 CONC CUTLET GAS

N2 INLET VCL FLOW RA'fg
N2 INLET VCL FLOVi RATE
N2 INLET VCL FLCVi RATE
Z TOT S ON INLET CA3'3Ch
% TOT S CN IN'LET CASeC!'.

S TOT S CN CUTLET CA16CN
Z TOT S CN CUTLET C«ECJ(
% H20 ON INLET CARBC-i
S H20 ON INLET CARBCV

% H20 ON CUTLET CAF-ECN
? H20 QK CUTLET CARECN
% ACIC ON CUTLET CAR2C!*
% ACID ON CUTLET G£R!=C:>
% ACID CN CUTLET CAREC.t
% iCIC ON CUTLET CA3ECA
% ACID ON CUTLET CARHCN
(GS-206) /
(GS-206) /
(CS-2C6! /
(GS-2CC) /
(GS-200) /
CGS-200) /
(GS-206) /
(GS-2C6) /
(GS-206) /

(GS-2CO) /
(GS-2CO) /
(GS-2CO) /
(GS-2C6) /
«GS-2C6) /
(GS-206) /
(GS-2CC) /
(GS-200) /
«GS-200> /

IGS-206) /
(GS-206) /
(GS-2C6) /
CGS-2CO) /
(GS-200) /
(GS-2CO) /
(GS-206) /
(GS-206) /
(GS-2C6) /

( G-2CO) /
< G-200) /
< C— 2CO) /
(CS-302! /
(CS-302) /

1CS-2CO) /
(CS-2CO) /
(CS-302) /
(CS-302) /

JCS-2CO) /
{CS-2CO! /
(CS-2CC) /
JCS-2CO) /
(CS-2CO) /
1CS-2CO) /
(CS-2CC) /
Y2C6(ltT) =
Y206IltT) =
AY206A =
Y200(2tT) =
Y200(2iT) =
AY200B "
Y206(2,T) =
Y206(2»T) =
AY206E =

Y200(3,T) =
Y2CC(3tT) =
AY200C =
Y206(3tT) =
Y2060.T) =
AY206C =
Y2CC(4,T) =
Y2COI4.T) =
AY200C =

Y206(4,T) =
Y206(4,T) =
AY206D =
Y200(5,T) =
Y20C(5,T! =
AY20CE =
Y206(5tT) =
Y2C6C5»T! =
AY2G6E =

G20C<;,T) =
G2CO(5,T) =
AG2COE =
Z302(UT) =
AZ3C2A =

220C(1,T) =
AZ20C* =
Z3C2I2.T) =
AZ302B =

2200(2, T) =
AZ200E =
Z2C013,T ) =
Z200I3.T) =
Z^OCOrT) =
Z2CCi3, 5 i *
AZ2CCC =
0.960
1.100
1.030
28.300
25.700
27.000
1.000
0.720
0.860

0.0
0.0
0.0
0.0
0.0
0.0
10.200
11.200
10.700

48.300
48.200
43.250
58.900
58.500
58.700
49.500
49.800
.49.650

180.000
180.000
180.000
8.200
B.200

24.000
24.000
7.350
7.350

0.240
0.240
0.940
1.210
1.310
i.iJC
1.140
? (VCLUHE)
* 1 VCLUME I
* (VCLUKE)
* (VCLUME)
X (VCLUME)
T (VCLUME)
% (VCLUME)
? (VCLUME)
S (VCLUME)

1 (VCLUME)
* { VCLUME )
? (VCLUME)
% (VCLUKE1
* ! VCLUM E )
S (VCLUME)
S (VCLUME) ' -•
? (VCLUME!
? (VCLUME)

? (VCLUME)
S. (VCLUME)
S (VCLUME)
? (VCLUME)
S (VCLUME)
S (VCLUME)
* (VCLUME)
? (VCLUME)
Z (VCLUHE)

CFH (7C CEG F)
CFH (70 DEC F)
CFH (70 CEG F)
? (WEIGHT)
? (HEIGHT)

? (V,EIC-nT)
S {V.£!GrT)
J (V.EIGHT)
% (WEIGHT)

S (WEIGHT)
.3 (XE:C-:-.TJ
" (WEIGHT)
? (WEIGHT)
% CnEIGHTJ
k ! ? t i u r T )
? (WEIGHT)
j

t'
',
1 1
i .
•3.
ill
..'

-k
7
' J
73
_y
^
-t
"
-,
W
ta
-
_
-.
-^
\
j.
„-
.,
-
^
.-
.S

.-
..
-
''

-------
                                                                                                                          2/26/73
                                                                                                                                      PAGE
                                                    H 2 S
                                                             GENERATOR /SULFUR
                                                                                                 STRIPPER
Si
ON
Cn
V
Ij
Jt
4" '
i!

i*!

I-.

v
>l
>!
:»
R

H

r-
*
7.'
n
f'i
i«
H
Li
P
P
P
y
P
P
i. 	
i**

iJ
.,
<...
..
.11: 8 HRS
15: 8 HRS
" 1:26 HRS

12:32 HRS
0:15 HRS
11: 8 HRS.
15: 8 HRS
1:26 HRS

12:32 HRS
0:15 H°.S


12:32 HRS
0: 15 hRS
12:32 HRS
0:15 HRS

13:15 HRS
19:15 H«S
1S15 HRS


12:15 HRS
16:15 H?.S
20:15 HRS
0:15 HRS
4:15 HRS

9M5 HRS
9:15 HRS


3:15 HRS

21:15 HRS






247.90 HRS tET)
251.90 HRS 1ET)
262.20 HRS (ET)
AVERAGE:

249.30 HRS (ET)
261.00 HRS (ET)
AVERAGE:
247.90 HRS (ET)
251.90 HRS (ET)
262.20 HRS tET)
AVERAGE:
249.30 HRS (ET)
261. CO HRS (ET)
'- V E R A G E :

249.30 HRS (ET)
261. CO HRS (ET)
AVERAGE:
249.30 HRS (ET)
261. CO HRS (ET)
AVERAGE :
25C.CO HSS -ET)
256. OC HRS (ET)
262. CO HRS IET)
AVERAGE:

249. CO HRS (ET)
253. CO HRS (ET)
257. CO HSS !ET)
261. CO HRS (ET)
265.00 HRS (ET)
TOTAL:
RATE:
246. CO HRS IET)
27C.CO HRS <£T)
TOTAL:
RATE:
C.O HRS (ET)
AVERAGE:

258.00 HRS (ET)
AVERAGE:





H2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CONC INLET GAS
H2 .CONC INLET GAS
"
H2 CONC OUTLET GAS
H2 CCNC CUTLET GAS
H2 CONC OUTLET GAS
M2 CCNC INLET GAS
N2 CONC INLET GAS
N2 CONC INLET GAS
N2 CCNC INLET GAS
N2 CQNC CUTLET GAS
N2 CCNC CUTLET GAS
N2 CCNC CUTLET GAS

H2S CCNC CUTLET GAS
H2S CONC CUTLET GAS
H2S CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CONC CUTLET GAS
H20 CCNC CUTLET GAS
N2 IKLET VCL FLOW RATE
N2 INLET VCL FLCW RATE
N2 INLET VCL FLOW RATE
N2 INLET VCL FLCW RATE

WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CCST
WEIGHT CYCLCNE CC'ST
WEIGHT CYCLCNE CCST
WEIGHT CYCLCNE OUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CUST
WEIGHT FILTER CUST
WEIGHT FILTER CUST
WEIGHT KILTER CCST
HEIGHT FILTER CUST
% TOT S ON CYCLCNE CCST
% TOT S CN CYCLCNE CUST

X TOT S ON FILTER OLST
% TOT S CN FILTER CLST





,,
58.000 ? (VCLUHS)
57.133 t (VCLUME) . :t
53.900 ? (VCLUHE) :j
53.500 ? (VCLUHE) ;:»
58.700 31 (VCLUHE)
Sji
28.300 ? (VCLUME) -.'
25.700 ? ( VCLUME) -
27.000 S (VCLUME) ' W
10.200 ? (VCLUNE)
11.200 S (VCLUKE) i,
10.700 ? (VCLUME) .-,
175.000 CFH (7C CEG F) :'*
175.000 CFH (7C CEG F) :-|
175.000 CFH (7C DEG f) -,
175.000 CFH (70 CEG F) ^
.,'
0.0 LB CUST
0.055 LB CUST :-3
0.070 L6 CUST - y
0.064 LB CUST i.'
0.066 LB CC'ST (J
0.255 L6 CUST -J
0:016 IS CUST/HR
0.0 LE CUST ^
0.0 LB CUST 0
0.0 LE CUST
0.0 LB CUST/HR ^
24.000 ? (WEIGHT) L!'
24.000 I (WEIGHT) d
•^
24.000 ? (WEIGHT)
24.000 ? (WEIGHT) ' - :;
'2
bi
..,
- 1
if

-------
                                                                                                                              2/26/73
                                                                                                                                          PAGE
                                                                  CARBON
ON
k 	 21:_15 HRS 258. CO HRS t ET ) S RESICUAL S CN CARBCf.
'. AVERAGE:* RES 1C
'' 	 21:15 HRS 258. CO HRS 
UAL 3 C
UAL H2C
L'AL_H2C
RECYCLE
RECYCLE
S U L
N CARBC;,
CN CAR-r:N
ON CAR !CI*

RATE
RATE
FUR CON
 -i
5* -•
'
** . a

bo »
3: —
p*
bi


















^
r*

-------
                                                                                                                          2/2e/73




                                      STATUS  REPORT  CF  OPERATING CONDITION'S FCR  INTEGRATED  OPERATION OF S02 RECCVERY PROCESS
hJ

i —


_
•

i.
OPERATING FiRISD:
CATE: 2/26/73 TIME CF RECCRC
CAT£: 2/27/73 TIME OF RECCRC

PRCCESS ELAPSED TIKE CF PERIOD:
: 9:15
: 0: C

H*J TC 24: 0 HRS
H3S TO 9:15 HRS


,
s
START 246. (C hRS / END 270.00 f-RS LENGTH CF PERIOD: 24.00 HRS
SLyfiRY CF INTEGRATED PRCCESS PERFORMANCE:

S02 REHCVAL.

PRS02 =

S3. 71 X (ACTUAL) 90.0 % (GCAL)
I
•^
•'.
r ' ::
1 *•
•-• 3.
•i
- 4.
3
*: 5.
= 6.
rs
7.
r~\
3.
•» 9.

H2S UTILIZATION
ACID COVERSICN (TO SULFUR)

H2 LTILIZiTICN (TO H2S)

SULFUR RECOVERY
t-2 UTILIZATION 4" UNIT

RESIDUAL SULFUR ON CARBON
CiRSCN RECYCLE RATE (28)
—ACID LCACING INLET Ci.ReCN 6" UNIT

•--' 10. fOISTURc 'CONTENT INLET CARSON fc" UNIT
i- 11.
al 1?.

13.
14.
» 15.
r1 '•
,
'2

•*;
ACID LCiC!V3 INLST CiRECN 3" UNIT
_fOI.STURr *CNTENT_ INLET CARBON 8" UNIT

TOTAL ACIC CONVERTED 8" UNIT
SL'LCL-S CCNVEKSiO'.1 (TO H2S)
SULFLR CCNCENSER EFFICIENCY


V4JCR EVENTS DURING CPERATIMG PERIOD:
iT START OF PERIOD CUT h2 FLOVi TO
FUV2S »
PVCS -

FhCKS =

PRS =
PUH2 =

X90A =
RC90 =
X301C =

X3018 =
X302C =
X3023 =

PVC =
PSCHS =
£R\'4CO =


120 CF!-.
96.23 * (ACTUAL) 95. C * (GCAL)
87.96 5 (ACTUAL; 99.0 $ ;GCALI

69.39 S (ACTUAL) 90. C * (GCAL)

77.43 Z (ACTUAL! 100.0 % (GOAL) CF SCR8EO SQ2
21.64 % (ACTUAL) 25.0 * (GOAL) OF STRIPPED SULFUR
ICO. CO Z

C.C331 L8 S/L5 C
;:9.91S LB C1CB1/HR
0.2453 L3 ACIC/ie C
•
(i.lC14 LB S2C/LS C
c.2453 Lb ;::C/LS c
C.1C14 LB H2C/L6 C

93. SC %
77.72 S
97.14 S


FRC!' 132 CFH
••
-„
•-•
r
*;!
-;
:i
14
"5
J
'-J
-^
'-•=
^
;s
;._,'
3
..
t.
•_v
-

-------
                                                                                                                           2/26/73

                                      STATUS  REPORT CF OPERATING  CONDITIONS FCP. INTEGRATED OPERATION  OF S02 RECOVERY PRCCESS
                                                                                                                                        PAGE  S
                              OPERATING PERIOD:
                                  _EALE_:	2X 2 6 /13_
                                  _CAT£:   2/2.7/73_
jrjM£ OF RECORD:   9:15  MRS. TO  24: 0 HRS
 TIKE OF RECORD:	0:  0  t.RS  TG	9:15 HRS
                                   PRCCESS  ELAPSE^..TIX-E CF PERIOD:	S_TART__2't( .CC HRS /gNC   2'70.CO"t-_RS	LE-NC-TH CF PERIOD;    24.00 HRS
                              SULFUR MATERIAL  6A(.ANCE (USING PRCCESS  H2S1:	
                                                                        S 0 2
                                                                                _S C R S E R
                                       I N
                                              INLET GAS _A_S_S02
                      t  G- 13)  /  BG10A =
                                               2.5609  LE SULFUR/HR
N>
CT>
00
I
1
t
\
i
;
.
•
c
i
1
j
I
,.
I
I
!
*
t
i • — " "" ' •"
3
INLET C AS RESIDUAL
TOTAL

CUT
OUTLET GAS AS SC2
CUTLET CARBON
CYCLONE OUST
COLLECTOR DUST
CARSON hEEPAGE
TOTAL 0
6" D I A

I N
INLET CARBON
TOTAL
CUT
OUTLET CARBON
CYCLCNE OUST
TOTAL C


I N
S ( C- 1 1 i I
I N : (RV- 1C) i

{ G- 13 ,
( C- 12 t i
< 0- 111 i
< C- 12) i
(Cfe- 121 -
U T : (RV- 1C!' i
CARBON PR


t C- 12i .
I N' :  ,
U T : (RV-3CCI i
SULFUR G 1: I

,
' BC11A =
' SI10 =

r BG13A =
' 8C12A =
' BD11A =
' BD12A «
f BCU12A <•
' S010 =
E C 0 N D I T


I BC12A «
' SI 300 =

1 BC201A =
f BD301A =
t SO 300 =
•i E R A T C R


C.?8B9
3.5498

0.1610
3.3849
O.C186
C.CU9
O.CC08
3.5772
I 0 N E


3.3849
3.3649

3.3849
0.0
3.3849



LS
L6

LS
LE
LE
L8
LE
LE
R


LE
LS

LE
L8
LB



SULFUR/HR
SULFUR/H3

SULFUR/HR " •- ?
SULFUR/HR -.:
SULFUR/FR r
SULFUR/HR -,
SULFUR/HR . r
a

•
3
SULFU3/HR :
SULFUR/HR - -
-^
SULFUR/HR -
SULFUR/HR a
SULFUR/HR -
•«
,
-:
                                              IMLET GAS AS H2S  (CYL)
                                              INLET GAS AS H2S  (PRCC)
                                             _^ '- EI_CIR_B ON
                                                     T C T A  L
                                                                   1  N ;
                      {  G-2C1I / SG201B
                      <  G-2C1i / BG203R *
                     J_<>2C 1 I_/_BC201 A '
                      (RV-2CCI /  SI200 =
                                                        6.6729  L*  SULFUR/HR
                                                       __3.3349_LB_SULFUR/hR_
                                                       10.0579  LE  SULFUR/HR
                                     CUT
OUTLET GAS  AS  t-2S
OUTLET GAS  AS  SC2
CUTLET CAR3C.N
                                                   T C   A L
                                                                 OUT
                                                                             ( G-2C5 I / BG205B  =
                                                                             ( G-2C5 i / 3C-20SA  =
                                                                            _L_C- 2 C 2_)_/_B C 2 0 2A_y
                                                                             (RV-2CC I /  ~S0200  =
                                               0.2513 L2 SULFUR/HR
                                               C.3010 LE SUS-FUR/hR
                                               9.5749 LB SULFJR/i-R
                                              10.T271 L"e SULFUP'/HR

-------
                                                                     2/26/73
                                                                                  PAGE
H 2 S
         GENERA -TOR
                                    FUR
                                             STRIPPER
1;
• !
s'
.
':
i

*•

i
T,
r
I
^
a
•i
t*
J
„
„'
12
1
3
„;
•I
a
"

n
i
ij
J
J
•*•
J
1 N
INLET CAR8CN
T C T A L IN:

CUT
OLTLET CARBON
OUTLET GAS AS H2S
CUTLET GAS AS S
CYCLCNE CUST
FILTES CUST
TCTAL OUT:
OVERALL

I N
INLET GAS 18" UNIT AS SC2
INLET GAS 8" UNIT AS CYL H2S
TOTAL
CUT
OUTLET GAS 18" UNIT AS SC2
CYCLCNE CUST 18" UNIT
COLLECTOR DUST 18" UNIT
CARBCN ViEEPAGE 18" UNIT
CYCLCNE CUST 6" UNIT
CUTLET GAS 8" LNIT AS H2S
CUTLET GAS 8" UNIT AS SC2
OUTLET GAS 4" UNIT AS K2S
CUTLET GAS 4" UNIT AS S
CYCLCNE DUST 4" UNIT
FILTER CUST 4" UNIT
TOTAL S


.








{ C-.1C2)
(RV-iC C)


( C--.C3)
I G-U4!
< G--C4!
< C-U.1)
( C-U21
(RV-iCC)
S t L 1 U


1 G- 1CI
( G-2C1I
s u L r u

( G- !3)
< D- 11)
« C- 12)
(CV.- 12)
t C-3C1)
G-2C5)
G-2C5)
G-K4)
G-K4)
D-1C1)
0-1C2)
U L F I A











/ BC202A
/ snoo


/ SC103A
/ 6G104E
/ SC-.104S
/ eoioiA
/ BD102A
/ S0100
R B A


/ BG10A
/ 8G201B
R I N

/ BG13A
/ SOUS
/ 8012A
/ ECW12A
/ E0301A
/ BG205B
/ 8G205A
/ BG1046
/ BG104S
/ BD101A
/ B0102A
OUT












=


:s
=:
Si
=
=
L A


-
:

s
s
3
^
S
X
=
=
:











9.5749
9.5749


C.9889
6.6729
1.8583
O.CC38
0.0
9.5240
N C E


2.5609
0.0
2.5609

0.1610
C.0186
0.0119
0.0008
0.0
0.2513
0.3010
0.0
1.85S3
0.0038
0.0
2.6067











LE
LB


LB
LE
LB
LB
LS
LB



LB
LB
LE

LE
LB
LB
LB
LB
LE
LB
LB
LB
LB
LB
LB











SULFUR/HR
SULFUR/HR


SULFUR/HR
SULrUR/H.R
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/HR



SULFUR/H.R
SULFUR/HR
SULFUR/hR

SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/H.R
SULFUR/HR
SULFUR/HR
SULFUR/HR
SULFUR/KR
SULFUR/HR
SULFUR/HR
SULFUR/HR











-
'.
• i
•
;"l
r
'3
't
»y
-5
**
""!
v«

„
* n
s*
H
ri
•^

3
iu
bJ
c.
1
w
, t
•1
J
«J
*9
—
J
J
'";

-------
1 1
'.!
I-' .
'»;
(i
. I 	 	 	
i-
i"
u:
HYDRCGEN ."ATE3IAL BALANCE:

I N
INLET
IXLET
INLET
i^LET

S U

GAS AS H2
GAS AS I-2S (CYL)
GAS AS H2S (PRCC)
GAS AS r20
CAR3CS
TCTAL I N
L F I/ R i; 6

( G-2C3)
*< C-2C3)
! G-2C3)
( C-2:3)
', c-2;u
: IR\-2CC)
N 6 R /» T C

/ 3G2C3C =
/ BG2C3B =
/ 8G203 =
/ BC-2030 =
.' BC2Clh =
/ HI2CO =
R

C.O
c.o
0.4170
C-U52
C.4869
1.0691

LE
L2
t- r- r-
ru ru m
LS
2/26/73 PAGE 10


HYCRCGEN/HR
HYCRCGEN/hR
HYCRCGEN/HR
HYCnCGEN/r-R
HYCRCGEN/rR
HYCRCGEN/r-.S
i^
j)
:,
•.
•
i'
-,'
';! •.,'
?' CUT t»
r-
1 •
f1!
1.'


p
DLTLcT
Ci.;TLeT
OLTLcT
OUTLET
T


GAS AS H2
G1S AS H2S
GAS AS K20
CARBON
C T A L OUT

H 2 S GENE
{ C.-2C5)
. I C-2C5)
( C-2C5)
( 02:2)
: (RV-aiC)

R A T C f. / S
/ BG205C =
/ EG205h =
/ SG205D =
/ 8C202H. =
/ K12CC =

U L F U R
C.C
0.0157
C . S S C 9
0.0199
0.9166

STRIP
L8
LE
LS
LE
LB

P
hYCRCGSN/HR
KYCRCGEN/KR
HYCRCGEN/HR
hYCRCGEN/HR
HYCRCGEN/HR

E R
t
^
''•'.
:*
73
* i N y
•n
i
P
i.
£,'
i,'
H
ta

ES '
INLET
If.'LET
CUT
CLTLET
CL'TLET
CLTLET
1


GAS AS H2
CARSCN
TCTAL IN
GAS AS H2
GAS AS M2.S
GAS AS H20
C T A L OUT


< U-II3)
< C-2C2)
: (R'/-i:C)
C r,- 1 C4 J
( G-IC'V)
( G-IC4)
: ..; (R'/-1CC)


/ EG103C «
/ 8C202*- =
f nice =
/ EGIC4C =
/ EGlO^h =
/ BG.104D =
/ H01CO =


C.6C09
0.0199
0.6208
C.O
C.4170
C.1652
C.5822


LE
LE
LE
LB
LE
LH
Lfi


HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HS
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/H.R


•^
-4
1
-%
n
U.'
»'
• rr
•a
^
Si
=.' y
*_! • ' -j
H ' ^
»j> • ijc
'•*•' ~"
:_, ' -:


ij
I • ' ' - " • — • • — — - — -




























-
•1*

•-.
UV

-------
              APPENDIX A-12-3
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
        RUN IR-2-6  (37 - 51 hours)
                     271

-------
                                                                                                                              4/21/74

                                       STATUS  REPORT CF OPERATING CONDITIONS  FOR 'NfEGRATEQ  CPER4TICN CF  SC2  RECCVERY PROCESS
                                                                                                                                           PAGE   1
                              C?E"-
Q
3
j|
,5-


0
I-'
(4
'-:
S02SCRBER -7
16: 2
18: 1:
22:15
2: 15
6:15
20: 32
22:15
2:15
6: 15
16:15
6:15


18:15
2: 15
1C: 15


20:26
21:26
22:53
0:45
2:15
6: 15

4:15
1 x : ! 5
HRS
HRS
H.RS
HRS
HRS
MRS
hRS
HRS
HRS
_hRS 	
hRS


HRS
HRS
r.RS


HRS
HRS
HRS
"RS
HRS
HRS

HRS
hRS
« ?C:15 HRS

it
^l



4:15

4:15
12: 15


HRS

HRS


33.60
39. CO
42.00
47. CO
51. CO
A V E
41.30
42. CO
47. CO
51. CO
A V E
37. CO
51. CO
A V E

39. CO
47. CO
55. CO
A V E

41.20
42.20
42. 6C
45.50
47. CO
51. CO
A V E
25.00
3 3. CO
41. CO
49.00
T
HRS (ET)
H'SS (ET)
HRS JET)
KRS (ET)
HRS (ET!
RAGE:
.-HRS..!E!> 	
HRS (ET)
HRS (ET)
H.RS (ET)
RAGE:
HRS (ET)
hRS (ET)
RAGE:

HRS (ET)
HSS (ET!
hRS (ET)
RAGE:

HRS (ET)
HRS (ET)
HRS i£T)
HSS (ET)
HRS (ET)
HRS (ET)
RAGE:
HRS (ET)
HSS (ET)
HRS (ET)
HRS (ET)
0 T A L :
RATE:
25. CO HRS <£T)
33. CO
T

HRS (ET)
0 T A L :

S02 CCNC INLET- FLLE GAS
S02 CCNC INLET ?LUE Ct~
SC2 CCNC INLET FLUE G£S
S02 CCNC INLET FLLE GJS
S02 CCNC INLET FLUE GiS
S02 CCNC INLET FLUE G££
S02 CCNC CUTLET FLLE G ' i
S02 CCNC CUTLET FLUE CiC,
S02 CCNC CUTLET FLUE G.':i
S02 CCNC CUTLET FLUE G/-".
S02 CCKC CUTLET FLUE G.-,';
H20 CCNC INLET. FLUE G.!.'.
H20 CCNC INLET FLUE GAf,
h20 CCNC INLET FLUE GAS

CRIFICE PRESSURE ORCP
CRIFICE PRESSURE CROP
CRIFICE PRESSURE ORCP
CRIFICE PRESSURE ORCP

ORIFICE TEMPERATURE
CRIFICE TE'-'PERATLRE
CRIFICE TENP'JRATURc
ORIFICE TEt-'PERATLSE
ORIFICE TEMPERATURE
CRIFICE TEPFERATV.RE
CRIFICE TEr-'FERATLRH
HEIGHT CYCLCNE CLST
w = 'C-:-T CYCLCN; CUST
HEIGHT CYCLCNE CLST
HEIGHT CYCLCNE CLST
' WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DUST
HEIGHT CCLLECTCR DUST
WEIGHT CCLLECTCR DLST
U=IGHT CCLLECTCR DUST
WEIGHT CCLLECTCR DUST

-------
                                                                                                                                 "i/21/74
                           12:15
                                         2J.CC  (-3S (tT)
                                         4S.GO  H=S iET)
                                        	TOT  .'. L :
                                         AVS
                                                rt.S  (fc'TL.
                                                HftS..(ET>_
                                                SAGc :
                                   HEIGHT CARBCN
                                                                     C-'?.2C.?-
TCT
TOT
                                         S G\ CYCUCNE CLST
                                         S CN CYCLCNE DL5T
 iCV- 12)
 CCV- 12!
JCV:- .12.
 ! C ii— 12

 t_ e- 11
J  DT. ll
 f  D- 11
                                            CH121T)
                                            CW12!T!
/ _c • 111, T }	f_
/_ C11 i 1, T !	»_
/     AClli   =
16: 15 H?.S
 6:15 i-SS
                                         27. CO  !-. E ! G H T )
                                                                     S  (WEIGHT)
                                                                     ;  (v.;i
NJ
          H
          f-
          f.

-------
                                                                                                                         4/21/74
                                                                                                                                      PAGE  3
                                                         C 1  A
                                                                  C A R B C N
                                                                                  PRECCNDITICNER
21: 15
i 1:15
1 5:i5

21:15
1:15
: 5:15
' 4:15
:' 12:15

> 16:15
6:15

HRS
HRS
HRS

HRS
HRS
HRS
HRS
MRS

HRS
URS

42. CO
* f f\ "i
*» C • U v
5C.CO
A V £

42.00
46.00
5C.CO
A V E
35. CO
3-.CO
T
37. CO
5 i . C 0
A V E
HRS
H.RS
P. 
( ET t
I :
(ET!
(ET)
G E :
% TCT S CN INLET CAREC?>
s TOT s c:\ INLET CAREC?.
4 TCT S Cf. I ".'LET CAScCN
J! T3T S CN PJLET C
'. D-3jl)
i D-3C1)
/
1
I

1
/
1
I
1
1
t
1
/
1
Z 3C 11 1 , T ) =
Z301 :i,T) =
Z301'.liT) =
A Z 30 1 i -

Z 20 1 t 2 1 T ) «
Z30i(2,T ! =
Z33i;2,T) =
AZ3012 =
COSOHTi =
C030KT) =
W0301 =
SD3CI =
D20i!ltT! =
C3Ci;i,T) =
AD 30 I i =
6.340
7.940
£.060
7 . 4 " 7

10.700
6.£OC
13. COO
10.167
0.0
c.o
0.0
0.0
0.0
;.c-
0.0
•j
?

r)
".
•
L£
LE
LS
LB
;
a
(Vi EIGHT)
(WEIGHT)
IUEIGHT)
('.EIGHT)
:t
(S, EIGHT) ':
(hEIGHT)
(hEIGrT)
CUST ;,
CUST
CUSi
(WEIGHT) -r.:
! nEIGHT)
(nSIGrT) ;•
S3

-------
NJ
--J
t


-, » •
1



>.;
>.•
I-


u
-i
:.:

U. '
a»
i»
H
ss
i*
23:50 HRS
5:33 hSS
20: IS HRS
1:15 HRS
8m 5 1J3 C
23:50 HRS
5: 38 HRS


20:15 HRS
1:15 HSS
S: 2 HRS


23:53 HRS
5:38 HP.S
20:15 HRS
l: 15 HRS
8: 2 HRS
23:50 HSS
5:38 r.RS


20:15 HRS
1:15 HRS
8: 2 HRS

44.60 HRS f=T)
5C,<-0 HSS (ET)
AVERAGE :
41.00 HSS (ET)
46.00 HSS iET)
c •} Q ^ U~? ' C~*~ \
AVERAGE :
44.60 HSS !ET>
5C.40 HSS (ET)
AVERAGE:

41. CO HSS IET)
46. CO HRS JET)
52.30 HRS 
52.30 HRS !ET)
AVERAGE:
SULFUR e
S02 CCNC CUTLET 'GAS
SQ2 CCNC CUTLET GAS
S02 CCNC CUTLET GiS
!-2S CCNC INLET GAS
H2S CCN'C. IMET GAS
r25 ~C"«C INLEI GAS
H2S CCNC INLET GAS
H2S CCNC CUTLET GAS
H-2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS

HZ CCNC INLET GAS
i-2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS

S-2 CCNC CUTLET GAS
H.2 CONC CUTLET GAS
r-2 CCNC CUTLET GAS
H20 CCNC INLET GAS
H20 CCNC INLET GAS
H20 CONC INLET GAS
H20 CCNC INLET GAS
H2C CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2Q CCKiC CUTLET GAS

N'2 CQNC INLET GAS
N2 CONC INLST GAS
M2 CCNC INLET GiS
N'2 CCNC INLET GAS
ENERATCR
1GS-206) /
{GS-2C61 /
. (GS-206! /
IGS-200) /
".GS-2C01 /
iff -jri n > /
' C; 5 — £.\* V 1 f
, (GS-2CC! /
(GS-206! /
JGS-206) /
(GS-206) /

(GS-2CO! /
(GS-20C) /
(C-S-2CO! /
(GS-2CC) /

(GS-2C6) /
 =
Y206(2,T) =
.AY206B =

Y200(3tT! =
Y2C:! 3-,~l =
AY200C =

Y206t3,T) *
Y2C6I3.T! =
AY20£C *
Y200(4,1 ) =
Y200(4,T) =
Y2CO(4,T) =
AY2CCD =
Y2C£C4,1 ) «
Y206(4,T; =
AY206C =

v>rnfc.Ti s
Y2CO(5,T) =
Y200(5»T5 =
AY200E =
4/21/74 PAGE 4
0.700 J (VOLUME)
0.990
C.S45
47.500
46.900
& 7 x t" *"*
47.200
7.500
5. 300
6.65C

~'"C.O ""
0.0
0.0
0.0

0.0
0.0
c.o
c.c
0.0
0.0
0.0
4S.OOO
49.SOO
48.900

52.500
53.100
52. SCO
52.50C
? (VCLUME)
\ (VCLUME)
? ( VCLUME)
% (VOLUME) :
0 ( vn UMF )
? (VOLUME)
7, (VCLUME)
3 (VCLUME) -5
S (VCLUMS)
-j
S (VCLUME!
S (VCLUME) «
S (VCLUME) -«
? (VCLUME!
•-
S 1 VCLUME)
I tVCLUXS)
Tt (VCLUME) »
Z (VCLUME) --
S (VCLUME) -,
S (VCLUME) i.
1 t VCLUME) rs
Z (VCLUME)
3 (VCLUME) r.'
Z (VCLUME)
is
S (VCLUME)
% ( VCLUM2) • -.
? (VOLUME) -
? 1VCLUME) K
W
3*'
f"
f ;
Ui
J'
-2
-1 '
H
*5
t
r*
*,*?
,4*
*•-
•i
i?
tL3
4-
9»
2 3 : 50 HR S
5:38 KRS
16:15 HRS
6:15 HRS

0:15 HSS
1:15 HRS
5:15 HRS


21:15 HRS
l:li HRS
5:15 HRS


21:15 HSS
5:15 HRS
44.60 HRS (ET)
5C.40 HRS (ET)
AVERAGE:
37.00 HRS (ET)
51. CO HRS iET)
AVERAGE:
45.00 HRS t£T)
46.00 HRS (ET)
5C.CO HRS (ET)
AVERAGE :

42. CO HRS (£T)
46. CO HRS (£T)
5C.CO HSS t£T)
AVERAGE:

4:. CO HSS..(ET)_
46. CO HS"lcT>"
sc.co HRS ;ET>
N2 CCNC CUTLET GAS
N2 CCNC CUTLET GAS
N2 OGNC CUTLET GAS
N2 INLET VCL FLOW RATS
N2 IN'LET VCL FLC* RATE
N2 INLET VCL FLCH RAT3
% TCT S ON IN'LET CARSCA
i TOT S CN INLET C*REC\
3 TOT S CN INLET CAS2:\

S TCT S CN CUTLET C.t?.:'.^
I TCT S CN CUTLET CAS5>
* TOT S CN CUTLET C«3:N
% TOT S CN CUTLET CARSON

? H2Q CN INLET CAR3CN
t u->-> "\ r * • ' T '•••:• <~K
ff f£.w v^<> ltiw'^1 V,W>uv«l*
« H2Q CN IN'-;* CARBON
1GS-206) /
Y206(5,T) =
IGS-2C6! / Y206(;,T) =
(GS-206) / AY206E =
{ G-2CO) /
! G-20C! /
f G-2CC) /
(CS-3C2! /
(CS-302) /
(CS-3C2) /
ICS-302) /

(CS-200! /
ICE-2CC) /
(CS-2T.C! /
4CS-20C) /

ICS-JC2) /
"CCS-3C2) /
CCS-3C2) /
G200(5rT) =
G2CC(5,T) »
AG2COE =
Ji02(ltT) =
Z2C2I1.T1 =
Z302(1,T) «
AZ302A =

Z20C(1, T) =
Z2t5Ca,T) =
Z2CC!l,Ti =
A2200A =

Z3C2!2,T! =
Z302!2,T; =
43.800
43.400
43.6CO
106. COO
IC6.000
1C6.COO
6.340
7.940
8.060
7.447

6.040
22.900
22.6^0
17.193

10.700
6 . j C 0
13. COO
3 (VCLUME) ^
? (VCLUME) »
CFK (70 CEG ft ^
CFH (7C CEG F)
CFH (70 CEG F) ,:
? (XEIGHT)
? (V.EIGHT) .:
* (ViEIGH.T)
? (HEIGHT)
_j
* (WEIGHT)
•H (V.EICHT)
2 («EIGhT)
Z (ViEIGHT) .,
cj
? (HEIGHT) ;«•
? (WEIGHT) '.',.

-------
A V E
v. 21:15 HRS 4?.SQ
('I 1:15 HRS 46. CO
!! - v 5: 15 HRS 5C.CO
'" A V f
«.
'"i 21:15 H.RS 42. CO
• 1: 15 hRS 46. CO
5: 15 H.RS 5C.CO
!• A V E
*
R A
HRS
HRS
HRS
R A
HRS
HSS
HRS
R A

G E :
t£T)
<£T)
IET!
5 E :

(ET)
!ET)
! ET )
G E :

Z H2C CN
; H20 CN
% H20 CN
S H20 CN
% H2C CN

* AGIO CN
% ACIC CN
* iCIC ON
? ACID CN

INLET .-CARSCN
CUTLET CAR8CV
CUTLET C/SR6CS
CUTLET CAREC\
CUTLET. CARSC1*

CUTLET CARE:K
CUTLET C4REZN
C'JTLET CARE;^
CUTLET C*RE>

ICS-302)
JCS-2CC)
(CS-2CC)
ICS-2CC)
 =
Z2CC!2iT) =
Z2CO(2,Ti »
AZ200E =

Z2C:(3,T) =
Z20C!3,T! =
Z200(3,T) »
AZ20CC -

10
<*/;
.167
3-700
1
1
2

0
o
r\
^
0

.^00
.100
.067
.073
. 370
.510
.318

!!/
%
%
<*
*:
4
„
j
t
J

74 PAGE 5 ;
(V.EIGH.T) y
(v, EIGHTS
(WEIGHT)
(WEIGHT)
.

-------
f
.
L
|;|
•!
';!
22:26
4:
14:

15
32
HRS
HRS
HRS

H 2
43.20 HRS !ST)
45. CO HRS !ST)
AVERAGE :
59.30 HRS (ET)
AVERAGE:
S GENERATCR/SU
H2 CCNC INLET GAS
H2 CC.NC INLET GAS
H2 CCNC INLET GAS
H2 CONC CUTLET GAS
H2 CONC CUTLET GAS
LFUR STRIPPER
 =
(GS-1CG)
(GS-1CO)
IGS-1C8)
tGS-lCE)
/ Y100J3.T) =
/ AYIOOC -
/ Y103(3,T) =
/ AY108C =
4/21/74 PAGE 6
49.400 % (VCLUME)
4-9.500
49.450
0.0
0.0
I
3
J
(VCLUME)
(VCLUKE)
(VCLUME)
(VCLUME)
1
j
i
!.:
•4
il
*! ' i
22:26
V 4:15
is


i
• $-


9*)
P
3T
L,'

~*
hi
S*
'.p
, _ ,___
'a;
!ri
»
G
2*
?
to
u-'
^
.=

14:
•
14:

14:

16:
6:


4:
12:
20:
4:



4:
4:
*

21:
1:
5:


32

32

32

15
IS


15
15
15
JLS


15
15


15
15
15

16:15
6:

HRS
HRS

HRS

HRS

J3.S 	
H?,S
HRS


H', S
HRS
HRS
hRS



HRS
HRS


HRS
HRS
HRS

HRS
15 H.RS

•
43.20 H'-.S (£T>
45. co :-s.s :ET;
AVERAGE :

55.30 HRS (ET1
AVERAGE:
55.30 HRS tET}
AVERAGE:

59.30 HRS l=T>
AVERAGE:
37.00 HRS (ET)
51. CO HRS !ET)
AVERAGE :

25.00 HRS 1ET)
33. CO HHS (ET!
41. CO HRS !ET!
49. CO HRS tET)
TOTAL:
RATE:

25.00 HRS (ET)
45. CO HRS (ET)
TOTAL:
RATE:

42. CO HRS 1ET)
46. CO HRS (cT)
5C.CO HRS (ET)
AVERAGE:

37.00 HRS IET).
51. CO HRS (ET!
AVERAGE :
N2 CD.NC INLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS

N2 CCNC CUTLET GAS
N2 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS

H2Q CCNC CUTLET GAS
H2C CCNC CUTLET GAS
N2 INLET VCL FLCV R*TE
N2 INLET VCL FLC* R4TE
?42 IMET VCL FLCV. RME

IsEIGHT CYCLC^r CUST
*EIGr7 CYCLCNc CcST
WEIGHT CYCLCNE OUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE CLST
VEIGHT CYCLCNE DUST

WEIGHT FILTER CUST
•«EiGi-T FILTER CUST
•isStGHT FILTER CLST
HEIGHT FILTER CUST

% TOT S CN CYCLONE OlST
Z TOT S CN CYCLONE OtST
S TOT S CN CYCLCHE CLST
% TDT S G,\ CYCLC.NE CLST

S TOT S CN FILTER DLT.T
% TOT S CN FILTER OLST
S TCT S C-N FILTER DLST
(GS-iCC
;GS-ICO
f GS-ICC

(Gs-ica
(cs-ioa
jGS-ica)
•GS-1C8)

( G s— i o a )
tcs-ica)
( G-1CO)
( C-JCC)
{ G-ICO;

! D-101!
! 0-101)
( 0-101)
r D-101!
( D-101)
( D-1C1)

f >•* 7 rj j *
( C-iC-2 !
( C-1C2!
( D-102)

{ 0-lCl)
1 0-101)
C 0-1C1)
! C-1C1)

{ D-102)
( D-1C2)
t D-102)
/ Y1CO(;,T) =
/ YlQOiS.T! =
/ AY10CE =

/ Y108(5,T) =
/ AY106E =
/ AY1CSE -

/ Y108(4,7) =
/ AY103D =
/ G100(5,T> •
/ G!CC(5,T! =
/ AGIQOE =

/ C010KT) =
/ CDlOliT ! =
/ CD 10 1(7) =
CD 10 1 ( T i =
/ wcici =
/ RD1C1 =

/ C01C2!7) =
/ CD1C21T) =
/ KCIC2 =
/ RD102 =

/ OlOHl.T) =
/ C1CK1.T) =
/ D10K1.T) =
/ ACL01A =

/ 0102(1, T) =
/ C1C2I1.T) =
/ A0102A =
5C.6CO
50.500
5C.550

55.200
55.200
35.000
35.000

7. £00
7.800
121.000
121. OCO
121.000

0.0
0.020
0.010
C.020
0.050
O.C02

0.0
0.0
0.0
0.0

2.720
3.200
3.640
3.137

0.0
0.0
0.0
&t s* w

%
S
S
?

%
?
I VCLUME)
(VCLUME)
(VCLU.XE)

(VCLUME)
(VCLUME)
(VCLUME)
(VCLUHE)

(VCLUME)
(VCLUHE)
't'
\3
!'i
!^
1
•g
'.-s
-.
•f.
^k
CFH (7C CEG F) W
CFH (7C CEG F) -,
CFH (70 OEG F) -

LB
Le
L3
L8
LE
LB

L3
IS
LE
LB

2
\

I
3
*

CUST
CUST
CUST
CUST
CUST
CUST/HR

CUST
CUST
CUST
CUST/hR

UEIGHT)
UEIGH.T)
I WEIGHT)
(V.SIGHT)

(HEIGHT)
IhEIGHT)
(HEIGHT)
'-~
'-i
H
n
L,'
1:1
TT
34
3
3A
?>
a
'**



-------
                                                                                                                                 W21/74
                                                                                                                                              PAGE
00
,„„

«!
ii!
•i
*,
i1
*
i
J
t
1
A,
4
r
*
PI
P

L.
t«:
f'~
P
sj
>>'
S
i*
as
U'

-it
*•'

^
B
0
CARBCN I IV V
21:15 HRS A?. CO HRS tfT) ? RFMC^At •> CM CARRf\
1--15 HRS 46.00 HRS (ET) % RESIDUAL S CN CARSC.N
5:15 HRS 5C.CO HRS (ET) % RESICUAL S CN CAR2CH
AVERAGE: * RESIDUAL S CN CARECf.

21:15 HRS 42. CO HRS (ET) % RESIDUAL H2C ON CARECiv
1:15 HRS 46. CO HRS (ET) % RESiCUSL H2C CN CARECA
5:15 HRS 5C.CO hRS ( ET ) ? RESIDUAL H2G CK CAREC^
AVERAGE: % RESIDUAL H2C CK CARGCIV
16:15 HRS 37. CO HRS (ET) CARBCN RECYCLE RATE
6:15 HRS 51.00 HRS (ET) CARBCN RECYCLE RATE
AVERAGE : CARBCN RECYCLE RATE
S U L F L R C C

Ifc:i5 HRS 37.00 HSS (ET) WEIGHT SULFUR CCLLEC1EC
6--15 KRS 51. CO HRS !ET) WEIGHT SULFUR COLLECTED
TOTAL: HEIGHT SULFUR COLLECTS
RATE: WEIGHT SULFUR COLLECUC









•

•




. .
ENTCRY HCPPER
!CS- 90) / Z90(1,T) =
.'CS- 50) / 290 (1-

-------
NJ
STATUS REPORT CF OPERATING CONDITIONS FOR
"i
3;
• •
OPERATING PERIOD:
CAT=: 4/21/74 TIME CF RSCCRC
CATE: 4/22/74 TIXE C~ RBCCRC
: 16:15 HR
: 0: Q H!:
IJvTEGRA
5 TO
S TC
4/21/74 . PAGE 8
TED OPERATION OF S02 RECOVERY PRCCESS
24: 0 HRS
6:15 HSS
i
:
.
'.' •
k.
PRCCESS ELAPSED TIKE CF PFRIH3:
START 37,
CC HRS
/ END 51. CO f-RS LENGTH OF PERIOD: 14.00 hRS
•' SUMMARY GF INTEGRATED PRCCESS PERFORMANCE:
—
;.

1. S02 REfCVAL

PRSC2 =

97. 7S

% (ACTUAL) 90. C ? (GCAL)
.
i'
t!
"3
,-r
,J • :.-
%
•r
:A
!•<
»
-?
2. r2S UTILIZATION
3. ACID CONVERSION ( TC SULFUR)

4. 1-2 UTILIZATION (TO H2S)

5. SULFL'R RECOVERY
6. (-2 UTILIZATION 4" UNIT
FVCS '

PHChS =

P«
PUH2 =
£•2.94
{.3.99

fcO.76

C.C
c.c
ICO. CO
S (ACTUAL! 95.0 * (GCAL)
% (ACTUAL! 99.0 ? IGCAL)

Z (ACTUAL) 90. C \ (GCAL)

S (ACTUAL) 100.0 % (GCAL) Or SCRBEO SC2
? (ACTUAL) 25. C \ (GCAU) OF STRIPPED SULFUR
3
'-i
4
ri
>

-»
?
:1
S3 " r*
:sj
r*\
(J
f -

w

B
•»
&5
1 1
ft
w
Li
P
t !
P
L
•J
7. RESIDUAL SULFUR ON CARECN
8. CARBON RECYCLE RATE (DS!
S. ACID LCADING i.\LET CARECN 6" UNIT

1C. ."OISTURE CONTENT INLET CARSCN 6" UNIT
11. ACID LCACING INLET CARECN 8" UNIT
12'. H.OISTURE --CKTENT INLET CAR8CN 8" UNIT

13. TOTAL ACID CONVERTED 6" UNIT
14. SULFUR CONVERSION (TO K2S )
15. SULFUR CONDENSER EFFICIENCY


PAJCX EVENTS DURING OPERATING PERIOD:
BY-PASSED 18" UNIT OUST COLLECTOR
X90A =
RC90 =
X301C =

X3018 =
X302C =
X3028 »

PVC =
PSCI-S *
ERV400=


37.0 HRS.
C.C337
;<,32i
C. 2134

C.. 1411
C..2134
C.. 1411

S8.15
i;!C.63
C.O



LB S/LE C
L8 C(OE)/HR
LB ACIC/L3 C

L3 H2C/L3 C
LB ACIC/L9 C
LB H2C/LB C

•it
%
%



'r,1

-t
-,
3J
"§
b^
t -
^

-".

•j
•*t
H
PLUS GAS STARTED 37.4 hRS. AT 3 FT/SEC.
CYLINDER I-2S TC £" UNIT STARTED 4C
.0 HRS.
L, H' TC 4" UNIT STARTED 40.6 HRS.; GAS VELOCITY


:'..G FT/ScU.
„,,'
' S
                                 CFF GAS 4"""LMT GCI.\G TO BURNER

-------
STATUS REPCP.T
f'; OPERATI'.G PtSTCC:
CATS: i/j.s/74
-
P.
..•t

I ft
•: INLET
:• INLET
•-
;i
C L- T
-. C-.TLET
i' CUTLET


GAS AS S02
c AS SESICL*L s
T C T A L IN:

GAS AS S02
CARSCN
•V y CYCLCNE CUST
Vf y CCLLECTCR CUST
v-> « CARECN
=s T
H
2*
W I N
pi INLET
'35
W ' C U T .._..._
r, CUTLET
V.ESPAGE
C T A L CUT:
6" 0 I A C A


CA33CN
T C T A L IN:

CA33CN
ic CYCLC.NE CUST
=- T
1 '
k>

- i IN 	
L- INLET
U ' INLET

,^,
CUT
-. OL'TLE i
V CL'TLET
• :- CUTLET
'.- T
C T A L CUT:
S U L


GAS AS H2S !CYL!
GAS AS r2S (PRCC)
T C T A_L I N :


GAS AS H2S
GAS AS SC2
CAS8CN
C T A L 0 U _T . :

s o 2 :
( G-
( C-
iRV-

! G-
/ r~
» V*
! C-
( C-
IC..-
(Rv-
R B 0 N


( C-
(RV-.

( C-
( C-.
(SV-
F U R


( G-
( G-
[ C-
!RV-



i : K B
13) /
11) /
1C) /

13! /
11) /
12) /
12) /
1C) /
P R E


12) /
:>co /

1! C 1 ) /
.1C I) /
:scc) /
GEN


iCl) /
2CC) /


? G-?C5) /
( G-2C5) /
I C-2C2! /
1P\-
2CC) /

E R
8G1CA =
BC11* =
SI 10 =

BCi3i =
3C12A =
BD11A =
B012/S =
BCW12A =
SO 10 =
CONDI


EC12A =
SI 300 =

8C201A =
60301A =
S0200 =
E R A T C R


6G2G1B =
6G203R =
3C2014 =
SI20C =


EC-2053 =
EG20SA =
8C202A =
S0200 =


2.
\s *
3.

0.
3.


A27£
9879
4157
0539
0312
C.01A6
0.
C
O.C051
3.
T I


3.
3.

3.
0.
3.



i .
C.
3.
10.


•> ^
r\
6.
7.
10A7
C N E


C312
02 12

0312
0
0212



3554
C
C312

1703
26CA
7710


L3
LB
L£
LB
IS
LB
* n
LB
"• *•
R


L£
IS

LE
L6
IE'

LE
L£
L;
L;
L=


SDLFUR/HR
SULFUR/HR
SLLFUR/i-R

SLiLFUR/hR
SL.'LrUR/1-R
SCLFUR/hR
SULFUR/HR
S(JLFUR/I-R
SULFliR/HR



SULFUR/hR
SLLFUR/rR

SULFUR/I-R
SULFUR/HR
SULFUR/i-R



SULFUR/!-R
SULFUS/HR
SULFUR/t-R
StLFUS/hR


suLFUR/sa
SLLFUR/.-R
SULFUR/i-S
SL'LFUR/HR
1
.-
1
: i
'.4*
•r
t
H
ri
;,
	 "
'-s1
-='
i!
.-!,'
_z
-^
=s
3-[
"1
3=
.5
*1
.:
.s
-.'
-.-
.3
•a
^

-------
                                                                                                                        4/21/74
                                                                                                                                    PAGE 10
OO

H 2 S G E \
ERATCR/SL
I N
INLET CAR30N


CUT
OUTLET
CUTLET
CUTLET
CYCLCNE
FILTEP
T


i M
TCTAL I


CAR3C\:
CAS AS h2S
GAS AS S
CUST
CUST
C T A L C U
0 V E R A


INLET GAS 18" UNIT AS
INLET GAS 3" UNIT AS
T C T
CUT
OUTLET
CYCLCNE

N :


-


T :
L L


SC2
CYL H2S
A L

GAS 18" UNIT AS SC2
CUST 13" UMT

COLLECTOR CUST 18" UMT
CAR2CN hEEPAGE 18" UMT
CYCLCNE CUST 6" UMT
CUTLET
OUTLET
CUTLET
GAS 8" UNIT AS
H2S
GAS 8" LN'IT AS SC2
GAS 4" UMT AS
OUTLET GAS 4" UNIT AS
CYCLCNS CUST 4" UNIT
FILTER CUST 4" UNIT






T C T A





H2S
S.
L S





{ C-2-:2)
(Rv-i :ci


I C-1C3)
( G-i:i)
( c-i:ii
i 0-1:21
tRv-i:ci
S U L F L


( G- 10:
( G-2C1:
S U L F L

< G- 13!
< D- 11!
( C- 12!

-------
                                                                                                                     4/21/74
                                                                                                                                 PAGE  11
                           HYORCGEN  MATERIAL
OO
N>
V

S U L F
*
UR CENERATC
R




!;]
IN . !.|
INLET
INLET
INLET
INLET
INLET

GAS AS
GAS AS
GAS'AS "
GAS AS
CAR3CN
T C T
H2
H2S 
(RV-i:O 1
' 5G205C =
' BG20SH =
' EG205C =
' BC202H =
' H02CO =

L F U R

' 8G103C =
' BC2C2H =
' H100 =
' BG104C =
' 8G104H =
C
0
C
0
*
•
•
•
0
0837
6158
C860
0.7855

S T

C
0
C
0
0


RIP
•
•
"
A
4921
0860
5781
0
3974
' 3G104C = C.C886
hOlOO
0
"
4860
LS
LE
LB
L3
LE

P E

L6
~L8
LE
LE
LE
LS
LE
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR

R

HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
KYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/HR
:->i
U
n
H
H
a
;j
•-i
H
18
'~i
^
H
:s
•J

-------
              APPENDIX A-12-4
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-2-6 (51 - 66 hours)
                     283

-------
oo
                                                                                                                        4/22/74




                                     STATUS REPORT OF OPERATING CONDITIONS F0:i  INTEGRATED OPERATION OF  SC2 RECOVERY PROCESS
                                                                                                                                    PAGE
                             OPERATING PERIOD:

V



'• _, pRre?*$ FI 4p<;=c Ti«f
-
i 	
;|
i;
'-
'•
\-*
.«

(
1
.-!
•
:
.^
nl
r

'i



PROCESS VARIABLES






10:15 HRS
14:15 HRS
18:15 HRS
22:15


11:15
15:15
18:15
22:15


6:15
21:15
HRS


H.RS
HRS
hRS
HRS


HRS
HIS



55. CD HRS
59.00 HRS
63.00 HRS
67.00 HRS
A V E R 4

56.00 HRS
6C.OO HRS
63.00 HRS
67.00 HRS
A V E R A

51.03 HRS
66.00 HSS
A V E R A


OF PERIOD: STAST JX.CC HI
..
f.1- LS





S
S02 CCNC INLET FLUE G,1S
S02 CCNC INLET FLUE G.sS
S02 CCNC INLET FLUE <5i»S

S02 CONC CUTLET PLUS CIAS
SQ2 CONC CUTLET FLUE GAS
S02 CCNC CUTLET FLUE CAS
S02 CCNC CUTLET FLUS GAS
S02 CCNC CUTLET FLUE CAS

H20 CCNC INLET PLUS G >S
H20 CCNC INLET FLUE SAS
H20 CCNC INLET PLUS MS

B E R

(GS-

49.00 HRS
65.00 HRS
T 0 T A
RAT

49.00 H^S
57. CO rRS
c5.CC rRS
(ET)
(=T)
L :
E :

(ET)
<£T)
(?T)
WEIGHT COLLECTOR OUST
WEIGHT COLLECTOR DUST
WEIGrtT COLLECTOR DUST
WEIGHT COLLECTOR OUST

WEIGHT CflRfiCN WESPAGE
WEIGHT C*RSCN WEcPAGE
WSICHT CAftBCf; WCEHAGc
c—
0-
0-
0-

(CV>-
(Cl>—
?Ci.-
12)
12)
12)
12)

12)
12)
12!
/ C012JT) =
/ C012(T) =
/ K312 =
/ R012 =

/ CW 1 2 ( T ! =
/ CW 1 Z ( T ) •
/ Cr.'12(T) =
0.0
0.0
0.0
0.0

0.0
0.060
0.040
LB CUST
L2 CUST
L3 CUST
L3 CUST/HR

LB CUST
LS CUST
L3 OUST
_,*
3
•3
ii
-M
.5

-------
f 	 — — - — • 	 • — • 	 	 	
I
I
f'l 12H5 HRS 57.
;=: 20:15 HRS 65.
I'j A y
i'l
'.>' ' 6:15 hRS 51.
21:15 HRS 66.
I'j A V
JJ:
r«i

?:!
M
TOTAL:
RATE:
CO
CO
E
00
CO
E




H»S IET!
HRS (ET)
RAGE:

K»S (BIT
HSS (ET)
RAGE:




WEIGHT CtRBCN WEEPAG!
XEIGHT CAR9CN WEEPAG1
S TOT S
X TCT S
Z TOT S

S TCT S
S TOT S
* TCT S




CN CYCLCN6
CN CYCLCNE
Cl\ CYCLCNS

C' ST
Cl.ST
Ol.'ST

CN CCLLECTCR CL'.iT
C\ CCLLECTOR CLIiT
CN CCLLECTOR CLST








(CVi-
{ C-
t 0-
( 0-

{ D-
C 0-
; o-




12)
12 )
11 !
11!
li)
121"
12 )
12!




/ WCH12 =
/ RCW12 =
/ 011(1. T) =
/ Cll(l.T) =
/ &011A =

/ 012(1. T) =
/ 012!1,T) =
/ AR 1 7 & —





4/22/74 PAGE 2 ]
0.100 LB CUST
0.006 L8 CUST/HR
S
6.080 %
6.800 %
6.440 %

C.O %
0.0 ?
0.0 %




(ViEIGHT)
(ViEIC-HT) j
(WEIGHT) •=

'.
(WEIGHT) .
("EIGHT) .
(KEIGHT) jrf
-•




••,
•:
:r'

K5
00
Ul
          C:

-------
                                                                                                              4/22/74
                                                                                                                         PAGE   3
                                                6"  0  I A
                                                            CARBON
                                                                          P R  E C C N C I
                                                                                           1 C M E R
oo
L
;'

:-'


•:
• \
)!•
H
!!.'
u.
It
'-;
52
-J
;t
£
:«
c*
-a1
3-
R.-,'


C*'
P"
i •
g 	
U
!-=;
 till S TCT
AVERAGE: 3 TOT

13:15 t-RS 5S.".C t-P5 SET) i H20
17:15 hRS Si.C: i-5S t=T) ? !-2C
21:15 !r WEIGI-T
20.-15 HRS 65. CC r-SS ! £7 '< KHIGS-I
TOTAL: X-£IC;-:T
T i T E : VvEICHT

6:15 "RS 51. CO >-SS !ET) S TOT
21:15 KRS 66. CO i-KS (ET) S TCT
AVERAGE: * TOT








*







s CN INLET C^RECN
S C\ 1NLST C-'TtC'
S C.N iMET CiS3C"
S CN INLET CiRDC":
S Ctv INLET CAS6C'-

CN INLET CASecN
CN l\LcT CAP.SCN
CN IM.ET CAK3CX

CYCLCNE DCST
CVCLCixE C'JST
CYCLC.NS OUST
CYCLIC DLST

S CN CYCLCNE OUST
S CN CYCLCN6 OUST
S CN CYCLONE ocsr
















?CS-3CU /

;cs-3cij /
(CS-301) /
t r £ "2^11 y
(C 5— 3C1 / /
iCS-iCI.) /
(CS-3C1) /
ICS-3C1) /
 =
fc-I«rf*i"»l) ~
Z3cI(i,T) =
6Z301A =

Z;01!2,T) =
230K2.T) =
1 30 1 ! 2 - T ) =
AZ30-E =

CD30KT! -
CC3CKT) =
«030i =
PC 301 =

03CK1.T) =
0301(1, T) =
AD301A *
















8.C80
7.920
6,<>OC
8.520
8.230

. 2CO
8.000
6.203
.8.000
S.100

0.0
0.0
0.0
0.0

0.0
0.0
0.0
















S HEIGHT)
S UcICrT)
S (WEIGHT)
t (kEIGHT)
J (kElGHT)
SI L/eifuTl
3 1V.EIGHT)
? (XEIGI-T)
S ti SIGHT)
i f«£IGHT)

LB CUST
IB CUST
L6 CUST
18 CUST/HR

% (HEIGHT)
S (kEIGl-T)
I (KEICHT)
















t

•,]
	 	 -- i4-

f
•.,
,.-;
•!
*'C
\.i
'•I


rj'
-^
t,

si
'•W

•i
. - 2*
	 	 	 -, t
5!
.4
H

11
'^
i
.M
                                                                                                                                         •^3

-------
to
co
i
i
\ 23:50 HRS
[•: 5:38 HRS
;! 21:32 HRS
i'i 	 ..•

= ?0:15 HRS
1:15 HRS
;' 8: 2 HRS
™ 23:50 HRS
.-s 5:38 HRS
>» 21:32 HRS
K , 20:15 HRS__
'•* 1:15 HRS
•T. 8: 2 HRS
'-' 23: 50 HRS
= 5:33 HRS
= 21:32 hRS
ri
S4
-- 2C:15 HRS
:-- 1 : 1 5 HR S
'=• 8: 2 HSS
zx
u.
* 23:50 HRS
= 5:38 hRS
:*- 21:32 HRS
'*'•
V ' 20: 15 HRS
* 1:15 HRS
=r S: 2 HRS
23:50 HRS
5:36 MRS
21:32 HRS
e . 1 C i^"N £•

21: 15 HRS
.-
..
9: 15 HRS
^ 13:15 HRS
'! 17:15 HRS
i: 21: 15 HRS
;
..
9:15 HRS
13: 15 HRS
44.60 HRS 
52.60 HRS (ET)
AVERAGE:
44.60 HRS (ETi
5C.40 HRS (ET)
66.30 HRS (ET)
AVERAGE:

41. CO HRS CET)
44. CO HP.S !ET)
52. SO HftS CET3
AVERAGE:

44.60 U'RS (ET)
5C,VD HRS (ET)
66-30 KRS 1ST)
AVERAGE:

41. CO HRS (ET)
46. CO HRS 1ST!
52.60 H^S (cT!
A V '- ?. A C- E :
44. tO HRS !£T)
5C.40 HRS (ET)
66.30 HRS (ET)
AVERAGE:
C 1 :* A S-. D f * £" \

66.00 H?S !tT)
AVERAGE:

54. CO HRS (ET)
58. CO H?S (ET!
62.00 i-kS ! ET)
66. -0 HRS !cT!
AVERAGE:

54. CC r-3 CET;
53. CO HRS (ET)
S02 CCNC CUTLET GAS
SC2 CCN-C CUTLET CAS
£02 CCNC CUTLET GAS
SC2 CCKC CUTLET GAS

H2S CCN-C INLET GAS
H2S CCNC INLET GAS
H2S CC\C INLET GAS
H2S CCNC INL3T- GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2 CCKC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H2 COiNC INLET GAS
r2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS

H2C CCNC INLET GAS
H23 COf;C INLET ^AS
i-20 CCNC INLHT GAS
H20 CCN'C INLET GAS

H2Q CCNC CUTLET GAS
H2S CO.\C CUTLET GAS
H2C CC?.'C CUTLET CAS
K20 CCr-.C CUTLET CAS

N2 CONC INLET GAS
?;2 CCfiC INLET GAS
^2 CO':C INLET GAS
1,2 CCNC INLET CAS
N2 CCNC CUTLET GAS
\2 CCNC CUTLET GAS
N2 CCNC CUTLET GAS
M2 CO.NC CUTLET GAS
- i -5 T v i "z T \ir". P t n \ ? i r *-

V2 IWL5T VCL FLCU RAtg
N2 "MET VCL FLCV. RATE '

S TOT S CN INLET CAR!CK
•4 TCT S CN INLET CA^:C!.
'i, TOT S G* INLET CAS"Ci>
% TOT S CN IML5T CAR:C!>
S TCT S C\ INLET CA=. iC,'.

•f, TCT S CN CUTLET CJ^KCN
% TOT S CN CUTLET CA>,£i::\
N E R A T C R
(GS-2C6) /
(GS-2C6) /
:GS-2Ct>) /
(GS-2C6) /


0.700 t (VCLUME) j
0.990 % (VCLUME!
0.980 Z (VCLUME) .:
0.390 S 1VCLUME) .1
.A
47.500 Z (VCLUME) :
46.900 J (VCLUME) .
47.200 ? (VCLUME)
47.200 S (VCLUME) '.
7.500 S (VCLUME) -»
5.800 3 (VCLUME) r.
4.450 Z (VCLUME) -,'
5.917 « (VCLUME) ™
0.0 % (VCLUME) "i
0.0 S (VCLUl'E)
0.0 S (VCLUME) -r
0.0 * (VCLUME) -,
0.0 J (VCLUME) r,
0.0 * (VCLUME) -.
0.0 S (VCLUME) n
0.0 * (VCLUMS) b
.<
0.0 S (VCLL'KE) -s
0.0 % (VCLUME) ;.
0.0 S (VCLUME) :-
0.0 ? (VCLUME) .-,
„
48.000 * (VCLUME) a
49.600 2 (VCLUKE) -,
51.800 % (VCLUME) =;
49.567 ? (VCLUMc) =j
.,
52.500 S (VCLUME)
53.100 ? (VCLUME)
52.cOO % (VCLUME)
52. £00 Z (VCLUME) -:
43.800 S (VOLUME) a
43.400 % (VCLUME)
42.800 * iVCLUME) .,
43.333 •? (VCLUHE)
T i f\ **"' ". n c P w f ~' ^ n c f* pi

1C6.CCO CFH (70 CEG F)
1C6.QOO CFH (7C CEG F)
t
S.030 S (WEIGHT)
7.920 3 (HEIGHT) .
S.^oo ? (V.S GHT)
C.fli; 7. (V
-------
                                                                                                                                          PAGE
to
CO
co
\ ....
•2-
!«•
-!1 . '
:•
Q 	
t-
•t
i.
K

i
::
-7
17: 15
21:15
9:15
12:15
17:15
21: IS

HRS
H?.S
HRS
HRS
hSS

9:15 :-*S
	 13=15 HRS
17-15 H3 S
21:15 HRS

9:15
13:15
17:15
2!:15




r-RS
HXS
HRS



62. CC
64.CO
A V =
54. CC
58. CO
62.00
6i.O j
i V r
	 5 5. CO
62. CO
66.00
t V £
54. GO
53. CO
62.00
66. CO
A V E


HRS (ET)
:-5S iETl
". ; G E :
. W( r
i/J i/* t/> VI «ip w> f> I
f*' »f 3* o' r1'. it t
J. 0. .1 .1. 0' .U ,L. ,
n^ i
rRS "
R fi C
^ * x
HSS
ET)
*"T )
ET )
£T )
E :
£T)
ET)
c • )
ET)
, E :
= T)
HSS (£T)
PRS (ET)
SAGE:


J TOT S CN CUTLET CJRE'.'.N
S TCT S CN CUTLET C/REIIN
S 7CT S CN CUTLET C^£CN
S 1-2C CN INLET C*RaC^
S H?0 CN I'.'.fT CiRUCV
X --2C C\ INLET C*R8C\
5 H2G CN INLFT- C^RBC1.
•i H2C e:; INLET c,KP,ac\
% H20 c*v CUTLET C^^SIN
2 H2C CN CUTLET CARB:K
! H20 CN CUiLET CARE -N
£ 1-2C CN CUTLET CASiiCN
S t-20 CN CUTLET CARHCN
t ACIO CX CUTLET CAs.C:,
S iC:2 CN CUTLET C*3cC:>
5 ACIC CN CUTLET C«*':Ci<
« ACiC C\ CUTLET CfSRCCIv
J iCID CN CUTLET CfiRECK


(CS-2CC!
ICS-2CO!
{CS-2CC !
(cs-^c^)
(CS-302 !
1CS-3C2)
tCS-302 J
ICS-202)
(CS-2CO)
«CS-2CO)
(CS-2SO)
(CS-2CC!
JCS-2CO)
iCS-2CCi
(CS-2CC1
(CS-2CO)
ICS-2CC)


't
r
t
i
i
i
i
t
i
i
/
t
/


7 200 ' 1 ? T ) =
Z2CC!i,T) =
Z302:2,T) =
:202!2.T) =
Z3C2(2tT) «
Z302!2,T) =
AZ302S =
Z20C12.T) =
Z200i2.T> =
Z20C!2,T) =
AZ20C3 =
Z2CO(2,T} =
Z2CC(2,T) m
Z2CO{3,T) =
Z2CC!3iT| =
4Z200C =


25.600
23.12C
24.210
8.2CO
S.COD
8.200
8.000
8.100
1.950
1.950
.SOP
1.40C
2.025
0.610
0.540
0.590
0.540
0.570


•v ey ov
;
J.
I

\
%
\


(WEIGHT)
( WEIGHT)
(KEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
I WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
f W-EIGHT)
(WEIGHT)




•.
«
,
i
.,
!r
>*
• t
"
•5
35
a'

> a
- ;«


-------
                                                                                                                     4/22/74
                                                                                                                                TAGS
N>
oo
.1
>i
*(. 22:26 MS
!'; 4: 15 HRS
I'j 14:32 HP.S
••
.
X: 22:26 <-RS
••-'' 4: 15 hRS
H
14:32 HRS
'•:T
'•; 14 = 32 HPS
?«,
!ij 14:32 HRS
•f
6:15 KRS
; 21:15 H3 S
—
b
:-! 4:15 KRS
=5 12:15 HRS
?•- 2C:15 HS.S
ti
»"* 	
ja 4:15 HRS
i:j 20:15 HRS
H
>
•>•• ' 9 : 1 5 HI S
=. 11:15 HRS
S-: 17:15 HRS
';! 21=15 HRS
f*
"• 6:15 HRS
H 21:15 hSS

i"=
f**"
1 '
'+'*-,
Ui
ILJ
W
• T -SS IET)
4S.CO HSS !£T)
A V E R 1 G E :

59.20 HRS (ET)
AVERAGE:
55.32 r-JS (s7)
- V i: ?. AGE:

59.30 HRS (ET)
AVERAGE :
SI.CO :-SS (ET!
AVERAGE:

49.00 HRS (ET)
57. CO HS£ (ST)
65. CO H=.S !£T)
TOTAL:
3 A T £ :

49.00 HRS (ET)
65.00 HRS (ET)
TOTAL:
R & T E :

54. CO HRS [ET!
56. CO HRS (ET)
62.00 HRS (ET)
66. CO HRS IET)
AVERAGE:

51. CO HRS (ET)
66. CO HRS (ET)
t 11 c o A C c -




S GENERATOR /SUL
H2 CONC IN'LET GAS
H2 CONC INLET GAS
H2 cose I.NLET GAS
!-2 CONC OUTLET GiS
H2 CQNC CUTLET GAS

.S2 CCNC INLET GAS
N-2 CQ\C INLET GAS
N2 CCKC INLET GAS

N2 CCNC CUTLET GAS
N'2 CCNC CUTLET GAS
!-2S CCNC CUTLET GAS
:-2S CCNC CUTLET GiS

H20 CCNC CUTLET GAS
H2C CCNC CUTLET GAS
N2 I.SLET VCL FLCW RAT-;
N2 IflLcT VCL FLC'.. SATl:
N2 INLET VCL FLCV. RATE!

WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE OUST
HEIGHT CYCLCN-E CLST
WEIGHT CYCLCNE CUST

WEIGHT FILTER CUST
WEIGHT FILTER CUST
WEIGHT FILTER DUST
WEIGHT FILTER DUST

% TCT S CN CYCLCNE BUST
% TCT S ON CYCLCNE CLST
% TOT S CN CYCLONE CLST
% TCT S CN CYCLCNE DLST
* TOT S CN CYCLONE CUST

Z TOT S CN FILTER DLS"
% TOT S CN FILTER OLS"
** TOT ^ ^ V Ff'7c^ f J I ^ "




FUR S T
(GS-1CC) /
IGS-1CC! /
IGS-1C3) /
(GS-108) /
(GS-10SJ /

(GS-1CQ) /
IGS-1CC) /
(GS-1CO) /

(GS-108! /
(GS-108) /
iGS-lCS) /
•GS-lC'3) /

IGS-10S) /
fcs-icei /
i G-1CO) /
i G-iCOl /
1 G-1C01 /

( 0-10!) /
I 0-101) /
! 0-1 CD /
: o-io i; /
( C-101) /

( D-102) /
! 0-102) /
{ D-102) /
( C-1C2) /

! D-101) /
I D-1C1) /
( D-101) /
( 0-101! /
! D-101) /

( D-102) /
( C-1C2) /
r .-*_7 o? i /




R ! P P E R
YIOO(3,T) =
Y100(3,T! =
AY100C =
Y103(2,T) =
AY10EC =

Y100(5,T) =
AY100E =

Y108(5»T) =
AY106E =
Y 108 i 2 , T ) =
AY10£8 =

Y1CSI4.T) =
AY108C =
G:OO:;,T) =
GiCO'.i.T) =
AG100E =

C010KT) =
CC10HT) =
CC1QKT) =
'..3101 =
RD101 =

C01021T) =
CC102(T) =
XD102 =
RC102 =

DIOlil.T) =
ClOKltT) *
D 101(1,1) =
ClOKl.T) =
A0101A =

D102!1,T) =
ClC2fl,T) =
AO"1 Cj? A =




49.400 ? (VCLUME) ;
49.500 S (VCLUME) ^
49.450 S (VCLUHE) ':
0.0 * (VCLUHE)
0.0 S (VCLUHE) ,:
t
• 50.600 S (VCLUHE) jr.
50. SCO ? (VCLUME) '.
50.550 3 (VCLUME) ' i,
.--a
55.200 S (VCLUKE) }•{
55.200 S (VCLUKE) ^
-y
35.000 ? (VCLUME) :.!
35. COO ? (VCLUKE) '-*
:»
9.100 ? (VCLUME) -;
9.100 ? (VCLUKE) -.1
121.000 CFH (70 CEG F) W
121.000 CFH (7C CEG F) '-.i
121.000 CFH (7C DEC F) *
ra
0.0 LS CUST '-i
0.059 18 CUST -_i
0.083 LS CUST :.
0.147 L3 CUST '~
C.CC9 LE CUST/HR W
w
0.0 LB CUST »
0.0 LB CUST ;:i
0.0 L3 CUST - a
0.0 tS CUST/t-R v,
•^
3.640 S (WEIGHT) :,'
3.800 * (WEIGHT) b.:
3.960 » (WEIGHT) U
3.920 ? (WEIGHT) y
3.330 ? (HEIGHT) Uj

0.0 3 (WEIGHT)
0.0 Z (WEIGHT) .,
OO ZfWFIftHTl -^

— '
''I
..'

-------
                                                                                                                                      PAGE  7
                                                                CARBON
                                                                                i  N  V  E
                                                                                          T  0  R  Y
                                                                                                     H  C  P  P  E  R
S3
vo
o
V
b



w
I j 	
SI
S;
i .
9:1= HRS S4.GO HSS (£T) Z RESIDUAL S ON CARBCN
13:15 HRS Sc.CO HK3 (ET! % RSSICUAL S CN CARKCiv
17:15 HRS 62.00 HP.S (ET) Z RESIDUAL S CN CARET*
AVERAGE: ? R6SICUAL S CN CARECN

9:15 HRS 54-00 HRS (ET) % RESIDUAL H20 CN CAVJCN
13:15 HRS 5S.OC HSS IET) I R = $!CU£i. H2C QN CA*:CN
17:15 HRS 62. CO HRS (fT) % RESIDUAL H2C CN CA*=CN
21:15 HRS 66. C; HRS (£TI % RESIC'JiL H2C CN' C/U5CN

6:15 HRS 51. CO HRS ( ET ) CARSC^ RECYCLE PATE
21: 15 HRS 66. CO rRS !£T) CAS20N RECYCLE RATE
AVERAGE: CA^SGN RECYCLE RATE
!CS- 90) /
(CS- 9C) /
!CS- 9C) /
(CS- 90! /
(CS- 9C) /

(CS- 90) /
ICS- 90 /
tCS- 90 J /
SCS- 90) /
t f c Qr> % /
ICS- 9C ) /
( C- 90) /
: C- 9 C ) /
Z93U.T) =
ZSCM.T) =
Z9CI1.T) =
Z90U.T! =
AZ9CA =

Z90(2,T) =
Z90<2,T> =
Z90!2,T) =
A 7 C i"^ O

C9C(1,T) =
C90:i,T) =
AC90A =
3.640
3.600
3.960
3.920
3.830

2.230
2.230
2.230
2.230
2-y -i n

31.000
31.000
31.00C
* (HEIGHT)
S (WEIGHT)
* (V.EIGHT)
? (V.EIGHT!
S (WEIGHT)

Z (WEIGHT)
3 (VvEICST)
J (WEIGHT)
S (WEIGHT)
- - - ~ "' — '
L8 fAT'L/HR
LS yAT'L/HR
L3 NAT'L/HR
^
:
,


I'

-r
<

--
SULFUR CC
N C E N S E R



-
r- t - ,
I*
s.

6:15 HRS 51. CO HRS (ET) WEIGHT SULFUR CCLLcCTSC
21:15 HRS 66. CO HRS (ET) fcEIC-H.T SULFUR COLLECTS
TOTAL; wEic-rT SULFUR COLLECT-EC
RATE: HEIGHT SULFUR CCLLECTEC
{ S-4C1) /
t S-«C1) /
t S-- 401) /
S40HT) =
S401 (T) =
ViSADl =
RS^Ol =
0.0
0.0
0.0
0.0
L8 SULFUR
L8 SULFUR
LS SULFUR
LE SULFUR/HR
;=
_
r? ~ ~
< , .
r* -»
f'

•









r*
IS
r* -=
A* ^
r._'
s«-
















±a
i<
=*
9. =.
* ;
( _

-------
VO
j
f:\
H
! 	
1*1
4:
i':'
f-


K. ...
H
V
a
£
3?
5-
'»*
K.
STATUS REPORT CF OPERATING CONDITIONS FCC
OPERATING PERIOD:
CATE: 4/22/74 TIKE OF RECC

PRCC5SS ELAPSEC TIfE CF PFRICD:

RC: £:15 It.
START 51 .

4/22/74 .PAGE 8
INTEGRATED OPERATION OF S02 RECOVERY PROCESS
S TO 21:15 KRS :'

CC_HRS
SUfKARY CF INTEGRATED PROCESS PERFORMANCE:
1. S02.3S.yOV.AL._.

. 2. V-2S UTILIZiTICN
3. iCIC CCNVS'.SIC'; < TC SULFUR)
4. h2 UT!L!ZAT!CM (TO H2S )

5. SUCFLS RSCCVERY
6. 1-2 UTILIZATION 4'-.tMT

7. RESIDUAL SUIFU» ON CARBCN

B. CARECN RECYCLE RATE (08)
«!. iCIO LC»;i'.t- :-;L>T CiRSON 6" UNIT
PRS02 =

PUH2S =
PVCS =
PHCHS =

FRS
FU't-2 =

X9QA =

PC90 =
-X301C =
96.56

84.73
99. C8
80.76

C.C
C.O
KC.CC

C.C408

25. 121
C.2213
!.
/ END £6. CO HRS LENGTH OF PERIOD: 15.00 HRS >-
,
i|
S (ACTUAL) 90.0 ? (GCAL) «
'<
X (ACTUAL) 95.0 S (GCAL) te'
f, (ACTUAL) 99. C ? (GCAL! .t
% (ACTUAL) 90.0 S (GCAL)
..j
3 (ACTJJAL) 10C.O J (GOAL) OF SCREED SC2 ,
g (SCTUiLi 25.0 S (GCAL) CF STRIPPED SULFUR ,;
% ':'
ri
LB S/LS C i,1

LB C!Ce;/KR :,•
LB ACIO/LE C y
ii :'.
-,
₯
y
3,1
~
-^
b
'«
1C. '--GISTUSE CC\T£',T !\LET CASBCN 6" UNIT

11. AC:0 LCACIKG IIJLST CAR8CN 8" UNIT
12. fOISTuRE CCM5N7 INLET C*R3CK 3" UNIT

13. TC-»iL iCiJ CCNV5RTSD C" UMT

14. SULFLR CC.XVERSIC^ (TC K2S)
15. SULFUR CCNCENSER EFFICIENCY

X3013 =

X302C =
X3C2B =

PVC

PSC1-S =

C.H12

C.2213
C.1I12

9&.49

75.53
0.0

L3 r2G/LS C -^
:J
«•*
LS ACIO/L8 C ;„'
LS H2C/LS C •:.'
-
% ;;'
^
S -r!
S
•• -'

MAJCR EVENTS DURING OPERATING P6RICC: .:.
L . PLUG IN GAS LINE FRCK 4" UNIT CYCLCNE 'J
i..: TG SULFUR r.nKn?hseR ACCOUNTED FCR Lj
W
k!

<•'
2C" i-2C PRESSURE CRCP .ACROSS CC.N
OLUG SLCV.N CUT AT 65. o HRS.
SWITCI-EO SACK ANC FCRTH BETViEEN'

CENSER.

BURNER AND S'J



1 FUR C

,
Ui
>
CNDEKSER CURING PERIOD. .j
.-:

-------
                                                                                                                             4/22/74


                                        STATUS REPORT CF  OPERATING CONDITIONS FCR  INTEGRATED OPERATION CF SC2 RECOVERY  PROCESS
                                                                                                                                         PAGE  9
V£>
OPERATING PERIOD:
TATF: 4/22/74 TIME C? RECORD

PROCESS =LAPSEC TIME CF PFRtCC:

SULFUR MATERIAL BALANCE (USING CYLI.NCER
: 6:15 H?S TO

START 51

H2S):

.CC HRS


21:15 HRS

/ END 66




.CO




HRS









LENGTH CF PERIOD: 15.00 I-RS


- i

til
!*!
;il
Lj

S 0 2
S C R 8
E R





!.-
: I N
i INLET GAS AS SC2
: INLET C AS RESIDUAL S
! T C T A L I N

: CUT
CUTLET GAS AS S02
CUTLET CASEC.N
CYCLCf.E 'CUST
i CCLLECTCR CUST
i CARBON V.EEPAGE
TCTALOUT
6 " C I A C A
! G-
! C-
: (RV-


! G-
< C-
( C-
( C-
ccv.-
: (RV-
R B C N
131 /
ill /
1CI /


i3l /
•.2! /
22) /
12) /
!C) /
- P R £
BG10A =
BCili =
SI10 =


SGI 3 A =
EC12A =
BD11A =
BD12A =
BCW12A =
S010 =
C 0 N C I
2
1
3


0
3
C
0
C
3
T I
.3304
.1873
.5177


.0602
.2914
.0181
.0
.CC07
. 3904:"
C K £
LB
LS
LE
LB
LB
LB
IE
LB
LB
R
SULFUR/HR
SULFUR/HR
SU'LFUR/t-R


SULFUR/hR '
SULFUR/HR
SULFUR/'rR
SULFUR/hR
SULFUS/r-R
SULFUR/hR

•f
\

.,
' 9
"
	 •_[
:~$
'-t

i rl
•IN -
. INLET CARBON
T C T A L I M
r- 1 1 T
t U U i
OUTLET CARSON
s . CYCLONE CU'ST
TCTALCUT
«: S U

I N
i INLET GAS AS t-2S ICYL)
INLET GAS AS !-2S (PSCC)
j • INLET CARSON
T C T A L I N1
( C-
: (RV-
( C-
{ C-
12 > /
3ftO) /
2C1J /
301) /
: (RV-3CC) /
L f U R


( G-
( C-
t; E N


2:)1 5 /
2^0) /
BC12A «
SJ300 =
BC2C1A =
BC301A =
S0300 =
E R A T C R


EG201B =
E-C2C1A =
SI20C =
3
3
3
C
3



7
C
3
11
.2914
.2914
.2914
.3 '
.2914


13554""
.0
.2914
.1468
LB
LB
LB
L3
LB

ia
* £X
15
L2
SULFUR/HR
SULFUR/h.R
S'JLFUR/hR
SULFUR /-HR
SULFUR/HR



SULFUR/rR
SULrUR/J-R
SULFUS/hR
SULFUR/HR
MJ
.*•;
^


TS
^.

-r
-s
JS
» **
CUT
,• OUTLET GAS AS H2S


( G-205) /

EG2G5S =

1
.1993"
L>

SULFUR/rR
-^
^
CUTLET GiS  AS  S02
OUTLET CARBON
     T CTAL     CUT:
                                                                               { C--2 ;2)  /  EC202A =
                                                                               (RV-2:c)  /   50200 =
 <;.60?S IS SULFUR/HR
10.9331 L2 SL.'

-------
VO
CO
       ci
t
;
I
!='
.«;
:
.' .
;j
. . — . 	 __
**", 	
l*
tj
•*
11
'i
~ 'r
.\
-=
;
J
y
t»
y
>
«
3^
it
H2S GENERAT
I f,
Jli'-HT CiP.SCN
T C T A L IN:

CUT
CUTLET CAR3CN
CUTLET GAS AS h2S
CUTLET GAS AS S
FILTER CUST
TCTAL CUT:
OVERALL

T *t
INLET GAS 18" UNIT AS SC2
INLET GAS 8" UNIT AS CYL H2S
TOTAL
CUT
OUTLET GAS 18" UNIT AS SC2
CYCLCNE DUST 18" UMT
COLLECTOR CUST 18" UNIT
CiSECN SEEPAGE 18" UMT
CYCLCNE CUST 6" UMT
CUTLET GAS 3" UNIT AS H2S
OUTLET GAS 8" UNIT AS SC2
CUTLET GiS 4" UMT AS H2S
OUTLET GAS 4" UMT AS S
CVCLCN£ CUST 4" UNIT
FT! TCIi ** * i C ^ A II i V T T

TOTAL S
0 "-( 1 S U
\ I-2C2!
{R J-1CC)


t >1C3)
( ,-lCl )
f :-iC2).
(Ru-lCC)
S L 1 F U


i •;- to
( 3-2C1)
S 1 L F U

( 3- 13)
'. 2- 11)
f S- 12)
(CV>- 12)
C 0-3C1!
5 3-2C5)
1 G-2C5)
{ 3-1C4)
! G-i'C4i
i c-icn
i r— i r 7 \

U L F U R
L F U R
/ 2CH02A =
/ SHOO =


/ EC1C3A =
/ EGIO'S =
C JiCl fi =
/ ec:o2; =
/ SC1CO =
R SAL


/ EG10A =
/ 8G201B =
R IN:

/ EG13A =
/ B011A =
/ 8DI2A =
/ BCW12A =
/ RD301A =
/ EG20SH =
/ 3C-205* =
/ 3G10-i8 «
/ 3G1C4S =
/ 8D101A =
t arii<~. 5A —

OUT:
STRIP
9.6073
9.6078


1.1873
6.3602
O.C
-C^04
C.C
7.5473
A N C E


2.33C4
7.S554
10.1853

0.0&02
0.0131
c.o
C.CC07
c.o
1.1998
C. 180=
6.3602
C.O .
C.CC04
0-p

7.8398
P

L8


Lfi
LS
IS
LE



LE
LB
LS

LE
LE
L6
L8
LS
L8
LB
LS
La
L8
L "

L6
4/22/74 PAGE 10
E R
SULFUR/t-R
SULFUR/HR
• ;
',
SULFUR/hR
SULFUR /HR ;
S'JiFUR/HR .:
SULFUR/HR :
SULFUR/hR

•5
f
SULFUR/HR
SULFUR/hR • -
SULFUR/t-S
.
SULFUR/hR :
SULFUR/I-R :
SULFUR/f-R :
SULFUR/I-R
SULFUR/HR ::
SULFUR/I-R :
SULFUR/hfi ;
SULFUR/I-R i
SULFUR/!-R ^
C 1 it C! I R /J-'P '

SULFUR/HR L

-------
                                                                                                                                    PACE  11
                              HYDRCGES MATERIAL BALANCE:
ro
vo

•

•
1


•-•
•i
ft
-
t
~.
si
*3
jj
C*


55

I N
INI FT
INLET
INLET
INLET


CUT
CUTLET
OUTLET
OUTLET
OUTLET
1


I N
INL5T
INLET

CUTLET
OUTLET



GAS AS
GAS AS
GAS AS
GAS AS
CAK3CM
T C T


GAS AS
GAS AS
GAS AS
CAR3CN
C T A

H 2 S

GAS AS
CASSCN
T C T
S U

H2
H2S (CYL)
H2S (PRCC)
ft L. IN


H2S
1-20

t OUT

GENE

H2
L F U' R

( G-;
( G-
( G-
1 G-.
( C-.
: (RV-.


( G-
! G-
( G-.
( C-
: !RV/-

R ft T C R

! C-
GE.NERATC

•C3)
:C3i
:C3)
:c3)


!C5J
!C5)
!C5)
!C2)
:CC)

• s u

.C3)
t c-:;c2>
A L IN
GAS AS H2
GAS AS
GAS AS
H2S
I-2G
: (R\<-
; G-
( G-
( C-
.CC!
tC^t)
.C1>
1C4)

/ 8G203C =
/ EG2C3B =
/ bG203 =
/ 8G203C =
/ 6C20IF =
/ S-I2CO =


/ SG205C =
/ BG205H =
/ 3G205S =
/ BC2C2H =
/ (-02 CO =

L F U R

/ 3G1C3C »
i 3C202H =
/ HI1CO =
/ BGlOiC =
/ HG104H =
/ 6C1C4C =
R

C.
0.
C.
C.
0.
0.


C.
C.
C.
0.
0.

S T R

C.
0.
C.
0.
0.
C.


f\
4906"
0
C
4914
9823

0750
6319
0939
SCO 7
I P
4921
C939
5S6C
0
3974
1033

LE
LE
LE
LE
LE


LS
LE
Te
ta
p
LE
LE
LS
.1-2
LE


HYCRCGEN/HR
HYCRC EN/hR
VYCRC E.N/hR
HYCRC EN/1-3
^YCSC ES/l-R


HYCRC EN/i-R
KYCc.CGEN/rR
HYCRCGE?;/HR
HYCaCGEN/rS
HYCRCGEN/VR

E R

HYCRCGEN/i-R
hYCSCGEN/1-R
HYC?.CGEiN/rR
MYCRCGEN/HR
HYCRCGEN/HR
KYCRCGEN/HS
• 	 -- ^^
'.
;!
,i

?

-:
i
•»
• s
"4

-|
1O
;,
r=
14
-"
:j
-,
:-
                                                    C T
                                                               OUT:

-------
              APPENDIX A-12-5
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
        RUN IR-2-7 (66 - 81 hours)
                     295

-------
                                                                                                                         4/22/7*


                                      STATUS REPORT CF OPERATING  CCNCITIONS FCR INTEGRATED OPERATION CF S02 RECOVERY PROCESS
                                                                                                                                      PAGE   1
N>
v£>
I
/T~ 	
I1:
i;'
!.!
]•• ....
!*-
J
1 _ _ 	 .__
V
»'




'

	 CAT?.- 4/22/74 TIME CF RECCRC: 21:15 H:S TO 24: 0
CATE: 4/23/74 T




PROCESS ELAPSFC fr^'?
PROCESS VAR!A9i = «:
IV.E CF RECCRC: 0: 0 t-f:S TC 12:15


CF PERICC: START tl ..CC HRS / END

HRS
HRS









.



1
J
\
»
•••.-
61.CC HRS LENGTH CF PERIOD: 15.00 HRS
FCR OPERATING PERIOD:
• ' *•>'
•i*

d
J*l

;•«
f'h
y
L-J
t»
H-
w
H
00
[j
U
y
J
r i
Id
U
!"i
r
P •
C



22:15
2:15
6:15
10: 15

22:15
2:15
6:15
10:45

21: 15
12:15


2:15
10:15
18:15

22: 2
0:20
4:15
7:20
10:15
12:15




HRS
HRS
HRS
HRS

HRS
HRS
HRS
HRS

HRS
HRS


HRS
HRS
HRS

HRS
HRS
HRS
HRS
HRS
HRS


20:15 HRS
4: 15 HRS
12:15 HRS






67. CO HRS
71.03 VPS
75. CO HR3
75. CO H?.S
A V E R A
67. CO HRS
71. CO HRS
75. CO HRS
75.50 HRS
A V t R A
66. CO .-RS
81.00 HRS
A V E R A

71. CO HRS
7S.CO HRS
S7.CC HRS
A V E R A

66. bO HRS
69.10 HRS
73. CO HRS
76.10 HRS
79.CO HPS
81.00 HRS
A V E R A

65. CC HRS
73.00 HRS
81. CO HRS
T 0 T A
RAT


(ET)
(ET)
(ET)
(ET)
G E :
(ET)
(£T)
(ET)
(ET)
G E :
(cT)
(ET)
G E :

!ET>
IET)
IET)
G E :

(ET)
(ET)
iET)
JET!
S
SC2 CCNSC INLET FLUE G,'!;
S02 CCNC INLET FLLE G.'S
S02 CCNC INLET FLUE GAS
S02 CONC CUTLET FLUE K IS
S02 CCNC CUTLET FLUE G.S3
SC2 CCNC CUTLET FLUE 0.!S
SC2 CCNC CUTLET FLUE >".!S
S02 CCNC CUTLET FLUE R,SS
H20 CCNC INLET FLUE G 55
H20 CCNC INLET FLUE G 5:5
H20 CCNC INLET FLUE G IS

ORIFICE PRESSURE DROP
CRIFICE PRESSURE DROP
ORIFICE PRESSURE CRCP
CRIFICE PRESSURE DRCP

CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE

WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE OUST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE CUST

B E R

4: 15
12:15
HRS
HRS


HRS
HRS
HRS
66.00 HRS
81. CC HRS
T 0 T A
RAT

65. CO H?S
73. CO HRS
SI. CO HRS
(ET)
(ET)
L :
E :

(tT)
<£T>
1ST)
WEIGHT CCLLECTCR DUST
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR DUST
WEIGHT CCLLECTCR DUS1

WEICHT C/SRFlCN V.££P4Gt
WEIGHT CARSCN HcSPAGF
WEIGHT CARBCN WEEPAGE
« D-
I D-
( C-
{ 0^

(CW-
(CW-
12)
12!
12!
12)

12)
12!
12)
/ CD12!T) =
/ CC12(T! =
/ WC 12 «
/ R012 =

/ CW12(T) "
1 Cwii'iT) »
/ CU1Z(T) =
0.0
0.0
0.0
0.0

0.0
G.C
o.cee
L8 CUST
L6 CUST
LB CUST
L8 CUST/HR

18 CUST
LE CUST
LB CU'ST
•3
'**
"J
•:A
-•»

-------
PAGE  2
1
''; 21:15
•'• 12:15
'•

i. 4:15
12:15
'i

HRS
HRS

HRS
hRS

T I
:
66.00
Sl.CC
A V E

73. CC
81. CC
ft V E
3 T i
* A '
H«S
a i

1-3 S

a A
fc i. :
r E :
1ST)
i£T)
G E :

(ET)
(ET)
G E :
«EIGH1
WE1GH1
?' TGT
Z TCT
* TCT

S TOT
S TOT
% TCT
r c
r c
S
S
S

S
S
S
:ARBC\' WEEPAGE
;ARBCN SEEPAGE
CN CYCLCNE OUST
CN CYCi-CN'E CLS1
CN CYCLCNE CtST

CK CCLLECTCR CIS"
ON CCLLECTCR CLST
CN CCLLECTCR CISV
ccx-
JCW-
< c-
< 0-
l D-

l D-
« D-
t 0-
12) /
12) /
11) /
li J /

12) /
12) /
12) /
WCVU2
RCW12
D1K1, T)
011(1, T)
iaiii

C12!1,T>
C12(1,T)
AC12A
a
=
=

s:
s
=
0.088
0.005
0.0
0.0
0.0

7.020
6.740
6.880
LB CUST j
LB CUST/HR 1
3 (HEIGHT) *.
S (hEIGHT) :
? (WEIGHT) :.
V
% (WEIGHT) :•:
S (WEIGHT) '.
* (WEIGHT) ;rj
                 _^ f

-------
                                                                                                                                            PAGE   3
                                                        6"  0 I A
                                                                      CARBON
                                                                                            COND
                                                                                                           ONED
NJ
VO
00
                         _l:15_H*_S_
                          5:15  i-'^S
                          9:15  H'.S
                          _5: 15  HRS
                          _9J-15_HR_SI
                          12:15  HRS
                         21:15 HRS
                         12:15 HRS
_7C.CO .H?-S_J.eTJ	
 74.CO HRS  (ET)
 7^.CC i-.'S  1ET)
 A V E R  i.  G j__:_

~7~4~. CO~HRS~( ETT)~
_78.CO HRS_JETJ	
 A V E"R  A  G E :
JB1.CO  HRS  (ETJ_
	T_0_!_ A L' ;_
	a  A  T E :

 66.CO  H?S  (ET)
 81.00  HRS  JET)
 A V E  RAGEi
 %_70T_S  CN__INLET__CAREC:.
~% TCT S"CN  INLET CiRiC.."
 % TOT S  CN  tMET C^RtC .
 z TCT s .cfv  INLET CARFCA

~% 7^2 H20 CN INLET CAR3CN  _
 Z I-"2C CN INLET CiRBCK "
                                                            >?IC-rT  CYCLCNE DLST_
                                                           J*E IGHT* CyCLCNE "CUST^
                                                            V.E IGr'T'CYCLCNE'CUST
 S TOT  S  CN CYCLCNE DUST
 t TCT  S  CK CYCLONE CU.'.T
 Z TOT  S  CN CYCLCNE OUST
(CS-3C1)
5CS-3C1)
ICS-3CI)
f CS-301}

 I , T ) =
Z3Cltl,T) -*
AZ3C14 =

Z30H2.T) =
Z301(2tT) =
AZ301E =
CD30KT) =
C0301 IT) =
VJ03C1 =
RD301 =
C301(1,T) »
D301U.T) =
AC301A *

8.880
S.S40
3.620
8.713

10.800
7.900
9.35C
0.0
0.0
0.0
0.0
0.0
0.0
C.O

i
1 (WEIGHT) }
? IWcIGhT) V:
S 1 HEIGHT) s'
'..
* (WEIGHT) •!,
? (XEIGhT) ..'
? (WEIGHT) ]>,
LH CUST :.|
LB CUST '.,'
LE CUST -t
L3 CUST/HR -;:
% (VEIGHT) .-^
J (WEIGHT) 'ij
? (WEIGHT)
•t
••,
»;
'a
-,
':«
        rv

-------
VO
I
I;
3S
*!
-.:
»;
7!
t
i

:»


'«J
-a!
sa
a1!
y
a
i.,
33;
^ 1
r*

'
31:
y
U



3*'
i i
cr,
L»


1 , — —
Us
U'
L"
.**
it ;
„,
i 	
u
a-.
i.
21:56 HRS
2:56 HRS
6:45 HRS

0:56 HRS
16:15 HRS
21:56 HRS
2:56 HRS
6:4= HRS

0:56 hRS
16: 15 HRS

21:56 Has
2:56 HRS
0:56 HRS
16:15 HRS

21:56 HRS
2:56 HRS
6:45 hRS


0:56 HRS
2:15 HRS


21:56 HRS
2:56 HRS
6:45 HRS
21:15 HRS
12:15 HRS

1--15 HRS
5:15 HRS
9:15 HRS


1:15 HRS
5:15 HRS
9:15 HRS


5:15 HRS
9: IS HRS
66.70 HRS (ET)
71.70 HRS tcT)
75.50 HRS !ET)
AVERAGE:

69.70 HRS (ET)
85.00 HRS (ET)
AVERAGE :
56.70 HRS !ET)
71.70 HRS (ET)
75.50 HRS icT!
AVERAGE:
69. 7C HRS (ET)
85..CO H-S (=T)
V c R A u c :
66.70 HRS (£7!
71.70 HRS !ET)
AVERAGE:
69.70 HRS (ET)
6 5. CO HRS (ET)
AVERAGE:
66. 7D HRS (ET!
71.70 t-RS (ET)
75.50 HRS (ET)
AVERAGE :

69.70 HRS !£T)
55. CO HRS !cT)
AVERAGE:

, t ~t f\ «'OC t ^"* \
66.70 rRS ( «: i )
71.70 HRS <=T)
75.50 HRS (ET)
AVERAGE:
66.00 HRS (ET)
81. CO HPS IET)
AVERAGE:
7C.CO HRS (ET)
74. CC HRS (ET)
73. CO HRS (ET)
AVERAGE:

7C.CO HRS (ET)
74. CO HSS (ETi
78. CO HRS  " r* \

(GS-2C6)
SGS-2C6)
(GS-2C6)
(GS-2CO)
(GS-2CO)
JGS-2CO)
{GS-206!
(GS-206)
(C-S-2C6)
iGS-2C5>

ICS-2CO)
(GS-2CC!
(SS-2CC!

t f  =
/ *G2COc »
/ Z302!1,T) =
/ Z302(1,T) =
/ Z302C.T) =
/ A23C2A =

/ Z2CO ! 1 e" ) «
/ Z2CC(1,T) -
/ AZ200A =

/ Z302I2,T> =
/ AZ3022 =
4/22/74 PAGE 4. j
1
1
0.950 J (VCLUME) J
1.210 3 (VCLUVE! iO
1.300 S (VCLL'KE) !:;
1.153 ? (VCLUKc) !=!

32.200 * (VCLUME) 1=1
27.200 ? (VCLUME! X
29.700 ? (VCLUME) -^
3.200 3 (VCLUME) i-i
0.700 S (VCLUME) -^
0.500 S (VCLUf.E) :i
1.467 S (VCLUME) >-j
0.0 S (VCLUHE) ''«'
0.0 ? (VCLUXE) -s
Of\ 5fV/f"IIIMPl •••

0.0 ? IVCLUME1 -i
0.0 ? (VCLUME)
0.0 I (VCLUf'E) »
14.000 I (VCLUfE) !=?'
21.200 « (VCLUME) r,'
17.600 J (VCLUME! :i
49.600 « (VCLUXE! -.'.
52.500 ? (VCLUME) *
52.9CO ? (VCLUME) T.
51.667 ? (VCLUMS) '-i
i>
53.300 ? (VCLUME) :,
51.100 S (VCLU.VE)
52.200 ? 1VCLUKE) -T
Z*
4*5 fif*O SfUPIIJMPl '-i

45.200 % (VCLUME) -^
45.000 S (VCLUME) '.-
45.333 J (VCLUME) ;.
121. COO CFH (70 CEG F) ..
121.000 CFH (7C CEG F)
121.000 CFH (7C OEC F) .,
S.8SO 3 (HEIGHT)
6.640 ?(» EIGHT) '...
S.620 S ("EIGHT)
8.713 i (WEIGHT! .
a
21.600 S (SEIGHT1
23.400 S (>.E:GH7!
20.20C ? IVEIGHT)
21.733 1 (HEIGHT)
.,
10.800 % HEIGHT)
7, f.;c T. C.EIGHT;
9.350 t (WEIGHT)

-------
U>
O
o
i l:
I I;
(^'
5:
9:
I 	 _
15
15
15
15
15
is'
HRS
HRS
HRS
HAS
HRS
HSS

7C.
74.
78.
i V
7C.
74.
78.
A V
CO
CO
CO
e
CO
CO
CO
F
HRS
HRS
HRS
R A
HRS
HRS
R A
(ET)
IET)
!ET)
G E :
(ET)
(ET)
•1ST)
G E :
% H20
% H20
% H2C
% ACID
% ACIC
% ACIC
ON
ON
CIS
HN
"CN
CUTLET CASECK
CUTLET CARECN
CUTLET CifEC
CUTLET
CUTLET
CA?.[
C
C

(CS-2CO)
(CS-2CC)
(CS-20C)
(CS-2CO)
5CS-2CC)
«CS-2CO)

-------
4/22/74
            PAGS

i'l
ij
t\
Ji
»i
ij
»;
1

22:56
13: 2
C: 8
4:56
0:38
22:56
13: 2

HRS
HRS
HRS
HRS
HRS
HRS
HRS

67.70
SI. SO
A V E
63.90
73.70
93.40
A V E
67. 7C
31.80
A V E
HRS
H*S
R A
HRS
HSS
HRS
R 1
HRS
HRS
R A
H 2

G E :
S GENERATOR'IU
H2 CCNC INLET G«S
H2 CCNC INLET GAS
H2 CCNC INLET CAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
LFUR STRIPPER
IGS-1CO) / Y100(3,T) =
(GS-1CC)
5GS-1CC!
JGS-108)
(GS-1CE!

ics-ioei
{GS-1CC!
;
S (VCLUNE) ;.,
3 (VCLUKE) !»
S IVCLUME) !.
S (VCLUKE) j'
S (VCLUKE) :-i
? (VCLUCE1 . -.,
s (VCLUKE) ••;
1 • '=?'
j
S
i!
0: 8
4:56
14:35

HRS
HRS

63.90
73.70
83. 4C
A V E
HRS
HRS
HRS
R A
(ET;
1£T)
(ET)
G F. :
N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
N2 CQNC CUTLET GAS

(tT!
G £ :
(ET)
(ET)
G E :
(ET!
(ET!
(ET!
A L :
T E :
!£T)
(ST!
ft L :
T E :

(ET!
!£T)
(ET)
G i :

(£T>
t£T)
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS

H2C CCNC CUTLET GAS
H2C CCNC CUTLET GAS
H2C CCNC CUTLET GAS
H20 CCNC CUTLET GAS
N2 INLET VCL FLOV, RATE
N2 INLET VCL FLC'« RATE
N2 INLET VCL FLCh RATE
HEIGHT CYCLCNE CLST
t-EIGrT CYCLCNE DUST
WEIGHT CYCLCNE DL'ST
ViEIGHT CYCLCNE CLST
HEIGHT CYCLCNE CL'ST
HEIGHT FILTER CLST
WEIGHT FILTER OUST
V.EIGHT rlLT;:' CUST
wcIGHT FILTER CLST

% TOT S CN CYCLONE CLST
% TOT S CN CYCLCNE CLST
% TOT S CN CYCLCNE OLST
% TOT S CN CYCLCNE DLST

S TDT S CN FILTER OLST
S TOT S CN FILTER OLST
S TCT S C;\ rIL~E* 3:.ST
{GS-106!
IGS-10E)
JGS-lOe)
(GS-103!

(GS-106!
IGS-103)
JGS-1CS)
(GS-108)
{ G-1CC)
{ G-1CC)
1 G-1CC)
( C-101)
; c-ici)
{ D-101)
( D-101)
( D-101)
t C-1C2)
! 0-1C?.)
( C-IC2S
! C-1C2!

j D-iOl)
{ D-101!
'. D-101 '•
i C-iCl )

i C-102!
; c-102 )
; D-102)
/
/

-/
/
~i
/
'\
1
1
/
1
1
J.

1
/
/
/
',
Y1C8!2,T) =
Y108(2,T) =
Y1C8(2,T) =
AY10E2 =

Y103(4,T) =
Y1C8;4,T) =
AY108C *
6100(5, T) =
G1CO! 5,T ! =
AG100E =
CD10HT! =
C01CK7) =
C010KT) =
WD101 -=
P.01C1 =
CC102IT) =
C01'J2(T) =
1.0102 =
RD102 =

CICm.T) -
0101(1, T) =
D101 Jl.T)' =
ADI CIA =

Ci02(l,7) =
SIC«102* =
34.400
32.900
29.600
32.300

11.000
14.100
19.500
14.867
221.000
121. CCO
121. COO
0.0
0.0
0.0
0.0
0.0
0.0
. 0.0
0.0
0.0

» (VCLUME) '-.
J (VCLUHE) V
% (VCLU.ME) u
? (VCLUNE!
12
Z (VCLUHE) ii
S (VCLUf-e) y
S (VCLUME) „•
? (VCLUHE) U1
CFH (7C CEG F) -,
CFH (7C CEG F)
CFH (70 OEG F) „
LB CUST i,
L8 CUST -3
LB CUST 3.'
LB CUST :j
LB CUST/HR „
LE DUST
L5 CUST
LS CUST
L2 CUST/hR
•„,'
5.160 ? (fiEIGHT) -J
5.230 2 ('"EIGHT! J
^.")73>

0.0
0.0
0.0
« I ViE. -.-T)
,-
a (WEIGHT;
* («EICHT)
* (HEIGHT) .,

-------
                                                                                                                                       PAGE
                                                                 CA1BCN
                                                                                 INVENTORY
                                                                                                     H C ? P E R
u>
o
•^
i;!

:•:
.1
£ i
t'l
*?
'-•.

fj
:'»
=
33
;7
-*
= •
r.
;.
,-
a
r
=-:
OS
=-:
I_J
r
1 ;
-4
V
L-
i • -
n~ '
	
U
r
J:

'•3

i
P
1:15 HRS 7C.CC HRS (ET) S RESIDUAL S CN CA*EC\
5:15 H3S 74. CO HRS (£7) % P.ESICUAL S C,\ CARECx
9:15 FRS 78. CO H-JS (ET) S SESICUAL S CN CAS6C,\
AVERAGE: Z RESICUAL S CN CAR£C\

1:15 HRS 7C_no PBS l FT ) « RESIDUAL H.2C ON CAS3CN
5:15 HRS T^.CO HRS IET) S RESIDUAL H2C CN C«;CN
9:15 HRS 73. 1C K^S (ET) i R£S:£UAi. K2C CX CAR3CN
AVERAGE: S RESICUAL H2C CN CAR2CK
21:15 HRS 66. CO HRS IET) CARSON RECYCLE RATE
12:15 HRS 31.00 HRS (ET) CAR6CN RECYCLE RATE
AVERAGE: CARfiCN RECYCLE RATE
SULFUR C C N

20:15 HRS 65. CO HRS f ET ) V.E1GHT SULFUR COLLECTED
23:15 HRS 68. CO HRS IET) HEIGHT SULFUR CCLLECTEC
3:15 HRS 72. CO HRS (ET) WEIGHT SULFUR CClLcCT^C
7:15 HRS 76.00 HI^S (ET) V.ESCHT SULFUR CCLUCTEC
11:15 HSS 3C.CO H-i.S !ET) USICHT SULFUR CCLLECT:.C
TOTAL: KEIGH.T SULFUR COLLECT =c
SATE: *EIGHT SULFUR COLLECT =c







*














XS- 9C> / Z / S«i(7) =
C S-'.C1) / SAOliT) =
• s-4Ci : / s'.oitT > =
{ S-^01) / i«S«i31 =
! S- / RS'iOl =


















•
•


5.160
5.2EO
3. S60
^.773

2.230
2.230
2.230
2.230
31.000
31.000
31.000


0.0
9.250
9.750
7.400
7.500
33.900
2. 260






















? (WEIGHT)
I (V.EIGHT)
1 (WEIGHT)
S C«EIGKT)

I ! nEIGHT )
? (HEIGHT)
% (HEIGHT)
LB PAT'L/HR
L6 KAT'L/HR
LE KAT'L/HR


L8 SULFUR
L8 SULFUR
LB SULFUR
LB SULFUR
LE SULFUR
L2 SULFUR
LB SULFUR/HR























•
•

i
.•3
.
..
•
-_

,
-
_

-^
«
-.
_
_
13
.^
IS

zs


.
-J
-S
«*.
^.
^
•=
-;
;,
U
>:

-------
                                                                                ~                                           4/22/74



                                        STiTUS REPORT CF OPERATING CONDITIONS  FC^i  I,\TEGRATED OPERATION OF S02 RECOVERY  PROCESS
PAGE  8
o
CO

r"- CPERiTIN3P?RICO:
I.,
pi GATE: 4/22/74 TI*£ CF RECCRC
i'1 CAT = : 4/23/74 TIKE CF RECCRC
: 21:15 t
: 0: 0 :-
: i
•RS TC 24: 0 HRS :
•RS TC 12:1= HRS

PRCCESS £LA?SEC TIKE CF PERIOD:
START fce.CC HRS / END 61. CO >-RS LENGTH CF PERICD: 15.00 HRS
;•: SUKXARY CF INTEGRATED PRCCESS PERFORMANCE:
ta
ft 1. SC2 REfCVAL
'",
H: 3. ACID CONVERSION ! 70 SULFUR)
?'
>>. 4. t-2 UTILIZATION ( TC H2S>
'-.i
!• 5. SLLFLR RECOVERY
f;
3'.
» 6. ^ UTILIZATION 4" UMT

PRS02 =

PVCS =

PI-CHS »

FRS
FUH2 =
'i
.
96.29 3 (ACTUAL) 90.0 * (GCAL)

94.31 Z liCTUii.) 55. C S -:CCAL)
81.66 % (ACTUAL! 99. C ? (GCAL) •-
\r
78.56 I (ACTUAL) 9C.C ? (GCAL)
-.
97. 4C -i (/.CTUAL) iCO.C S CC-CAL! OF SGS3HC SC2
33.20 % (ACTUAL: 25. c % (GOAD CF STRIPPED SULFUR
KO.CO %
pj ;i
tJ 7. RESIDUAL SULFUR CM CARECN
! t • ' "" , , ...
F--
» 8. C»RBON RECYCLE RATE IDE)
p 9. ACID LCACISC- IMLET CARECN 6" UNIT

W 1C. COISTURE CONTENT INLET CARBCN 6" UNIT
p 11. ACID LOADING IMLET CARECSv 8" UNIT
t- 12. "OISTURr CONTENT INLET CARSCN 8" UNIT
ps
i. 13. TOTAL ACIC CCNVEPTEO £" UNIT
;.-: 14. SLLFUR CCNVC-SSICN ITO H2S1
i
15. SULFUR CONDENSER EFFICIENCY

X9CA -
RC90 =
X301C =

X3013 =
X202C »
X3028 =

FVC »
PSCI-S =
EP.V40C-

C.C513 L8 S/LE C ;«
26.329 LB C(DS!/HR :,
C.2158 LB ACIC/LB C :t
T
C.1307 L3 h2C/LS C ;,
C.2158 L3 ACIC/LB C -
C.1307 L3 h2C/L6 C =.
,,
91.85 *
9C.89 % -,
364.24 S .;
,.
!.-' J2
'-•':• CAJCR EVENTS DURING OPERATING PERICC:
« ' S'niTCHEO TC PRCCESS H2S AT 66.4.HRS._
L V.ITH INLET PRESSURE AT 46" TC 52"
H20
43
.S
VI
I- SULFUR CONDENSER *>AS CN STREAH CURING PERICi:

-------
                                                                                                                  4/22/74     PAGE



                               STATUS  R=?C*T  CF  CPERATIN-G  CCNCITICNS FCR INTEGRATES CPERATICS CF 
PRCCESS ELAPSE
SULFUR V.ATFRIAI P.il 4K.

TIME" CF PERICD: STAR
CE (USING PROCESS H2S):

T " 46


.CC HRS


/ END '
-

SI. CO


HRS





LENGTH CF PERICC: 15.00 hRS


.

-.a
.•«. i
^3
£
U
-r

=:

I N
INLET
INLET


COT
CUTLET
S 0
GAS AS SC2
C AS RESIDUAL S
TCTAL IN:

GAS AS SC2
CAR5CM
CYCLCr.E CUST
UJ b
O L.
££
rs
?•
w

;.
-^
CCLLECTCR CUST
CAR2CN
T


I N
INLET
CUT
CUTLET
V.EEPAGE
C T A L CUT:
6" DIA CARB


CARBCK
TCTAL IN:

CAR3CN
2
t G-
( C-
(RV-

( C-
{ C-
{ C-
( C-
(C\—
(RV-
0 N


1 C-
(RV-

1 C-
5 C R 8
13) /
:ii /
! C) /

; 3 J /
12! /
; i ) /
12) /
12) /
!Ci /
P R e


1.2) /
3CC) /

2C1> /
=, CYCLCNE CUST ! C-3C1} /
'f.
'•47

^
A*
U
t '
•*fc
f : 	

'**•
v-
r 	
	
T


I N
5\L = T
INLET..


CUT
CUTLET
OUTL3T
OUTLET
T

C T A L CUT:
S_U L F U


C-fS AS H2S (CYL)
GAS AS h2S (PRCC1
CA.'.ECN
TCTAL IN:


GAS AS F2S
GAS AE SC2
CAP3CN
C T A L OUT:

-R
SULFUR/1-R
SULFUR/HP.



SULFUR/hR
StLFUR/S-R
SULFU-R/!-R
SULFUR/1-R


SULFUR/HR
SULF'JR/I-R
SULFUS/rR
SULFUR/h-R

-:
• t

-
' F
-"
3J
r:

"V
-,
-.,
:J

^
ti
-„
r3

.
-3
M
'-S
*i
--




• u

-------
                                                                                                                              4/22/74
                                                                                                                                           PAG= 10
                                                      H  2 S
                                                               G E N  E  R  A T C R /  SULFUR
                                                                                                    STRIPPER
U)
o
V.n
(,\ 	
H
;.!
•«•
-I;
'*

W" 	
\*
H
ti
I N
INLET CARBCN
T G T A

CUT
CUTLET CARBON
OUTLET GAS AS
OUTLET GAS AS
CYCLCNE CUST
FILTER CUST
T f T f 1
0

I N
INLET GAS IS"

L I


H2S
S

Ci |
V E R A


UNIT AS
••" INLET GAS S" UNIT AS
k . TOT
i;
f
»•


w
w
ti
y
n
0*
CUT
CUTLET GAS 18"


N :


-

Tv
L L


SC2
CYL H2S
A I

UNIT AS SC2
CYCLCNE CUST 18" UNIT
COLLECTOR DUST
C*?.ECN 1.CEPAGE
CVCLCN? CUST 6
OUTLET GAS 8"
OUTLET GAS 8"
CUTLET GAS 4"
OUTLET GAS 4"
CYCLCNE CUST 4
FILTER CUST 4"

18" UMT
IS" UMT
" UMT
UNIT AS
UNIT AS
UNIT AS
UNIT AS
" UMT
UMT
T 0 T A
SC2
H2S
S
L S
( C-.-'C?) /
1RV-':.CC) /


t c-:.C3) /
( G-'..^) /
( C- ' C 1 ) /
( c-:.c2) /
f o ti_ r r1 \ /
SULFUR


t G- 1C) /
( G-!C1) /
S U L FUR

( G- 13) /
I C- 31) /
t 0- 12) /
C5> /
< G-.2C5) /
( G-1C4) /
( G-1C4) /
i C-1C1) /
t C-1C2) /
U L f- U R
3C202A
SI1CO


BC103A
3G104-S
30 101 A
B0102A
C fl 1 i\ O
. B A


3G10A
3G2C13
I N

BG13A
8D11A
3012.1
8CV.12A
8C201 J
BG2058
BG205A
BG1048
BG104S
ED 101 A
BOi02A
OUT
S



"
-
=
1


—
:

—
X
S
8


1
6
2
C
C
A N C


2
n
\j
2

C
0
.2373
•'267T
.4797"
.1871
.2600
.0
-P. .
Q *) f- P
E


.4097
.0
.'iC97
.0893
.0
0.0
O.CC07
0.0
=
S
s±
S
i
0
0
C
.3245
.2552"
.C
2.2600
C.O
C.C
2
.9297
LB
LE


IS
L3
LE
L3
"f ft



LE
LB
L3
LB
LE
LE
LS
LS
L6
LB
LE
LE
LB
LE
LB
SULFUR/HR
SULFUR/HR


SULFUR/I-R
SULFUR/I-R
SULFUR/rR
SULFUR/!-R
SULFUR/I-R
C ! M Ft'I?/r

' i* ts J X - : i 2* ^' — — . t '31 =3 i^ M * .as a* P La' H 24 : t


-------
                                                                                                                     4/22/74
                                                                                                                                  PAGE  11
                       HYDROGEN  PATeaiAJ. BALANCE:
I** '" - - • _>
ill
i't— • 4 ...
i',! •• 	
\i
,'3-
;n
u
^ ;
li-



'.7
b
U
N
rs*
i*
'»
R

I N
INLET
I\LET
INLET
IMET
INLET


CUT
CUTLET
OUTLET
OUTLET
CITLET
T


I N
INLET
INLET
CUT
OUTLET
CUTLET
OUTLET
T


GAS
GAS"
S U L F

AS H2
AS H2S 1CYL)
GAS AS I-2S (PRCC) .
GAS AS 1-20
C4RBC.\
T r


GAS
GAS
GAS
T A L IN:


AS H2
AS H2S
AS H20
CA23CN
C T

H 2

GAS
A L OUT:

S GENERA

AS H2
CARBON
T C
GAS
GAS
GAS
C T
T A L IN:
AS H2
AS H2S
AS t-2Q
A L OUT:
U R GtNERATC

"1 G-.!C3) /
t G- >C3) /
!. G- !C2) J
( C— !C3) 1
t C-.JC1) I
(RV-.BCC) i


\ G-.K5! /
( C-~.C5! ;
i c-;?C2) >
(Rv-:?co i

T 0 P. / S U

( G- 1C3) /
{ C-2C2) 1
iRV- ico y
< G-IC4J i
t G-IC^) /
( G-LC4) t
iRV-LCC) ;

' BG203C
' EG2C3B
' BC201H
' H2CC


' 3G205C
' CC205i-
' SG2-05C
' BC202!-
' H020C

L F U R

' BG103C
' EC202^
' HI10C
' BG1C4C
' 3G104H
r 3G104C
' H0100

ts
= "
—
s
=


=:
R

C
0
C
C
C
1


C
0
C


.C
.C "
. 38"fcfc
.2113
.5457
.1436 '


.0
.2203
. 7 1 < 3
C.CS52
=



-
=

G

S T

C
C
C
.8193

RIP
.4921
.0352
.5773
o.c
ts
_
s:
0
C
0
-SB66
.1779
.5645

LE
LE
L2"
LE
LE
LB


LS
LE
L3
L6
LE
P £
L6
LE
LE"
LE
L6
LE
L8


HYCRCCEN/hR
HYCRCCEN/HR
HYCRCGEN/hR
KYCRCGEN/hR
HYCRCGEM/HR


KYCF.CGtN/HS
HYCRCG;:. /!-?-
HYCRCGEM/i-R
HYCRCGEN/HR

R

HYCRCGEN/I-R
HYCRCGEN/HR
HYCRCGEN/HR
HYCRCGEN/KR
HYC30G£.N/hR
HYCRCGEN/'rR
HYCRCGEN/rR
:;
.4
t
t


S3
4
1,

-,r
,
-
-,


-;
^
,,
33
:
w ^
;i
:






















«4
h






















-
.
i,' 	 "
•', .,
' 	 ' — «
>'--C

-------
              APPENDIX A-12-6
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-2-7 (81 - 96 hours)
                     307

-------
                                                                                                                        4/23/74



                                      STATUS  REPCRT  CF OPERATING CCNCITICNS FCF  INTEGRATED  CPERATICN  OF  SC2  RECOVERY  PROCESS
                                                                                                                                    PAGE
o
co
b
:*L
L;
*
;:-
P 	
ir
J
£ 	
P
fei
•31
3*'
[1
r»

»
£•'
•32
r***

k*
f !
W

ur
L'1
L- 	
i •
0
'•ux
y
u
H

Us
t ; "
S*

OPERATING P£R!CO:
	 	 CATE: 4/23/74
V
CATE: 4/24/74
TIME CF RF.CCRC:--. 12:15 i-?.!; T:
C 54: 0 HRS :'
TIME CF RECCRC: 0: 0 HRS TO 3:15
PRCCESS SLAP'SFC Tl'fF CF PFRTCD: START- PI .rr na<; / FKT
PRrcs.ss v:aiiP'p<; PTR PPI



15: S
18:15
22:15
2:15
15:20
18:15
22:15
0:32
2:15
12:15



HRS
HRS
HRS
HRS
HRS
HRS
HRS
HRS
HSS
3:15 HRS


18:15
2:15

• 14:32
16:26
19:15
21:20
l: 15
3:15


12:15
20:15
4: 15



12:15


12; 15
2C:15
4:15


HRS
HRS

HRS
hRS
HSS
HRS
HRS
HRS


HRS
HRS
HRS



HRS
HSS


H3S
HRS
HRS



33.90 HRS
67. CO HRS
91.00 HRS
95. CO HRS
A V E R A
84.10 HRS
67.00 HRS
91. CO HRS
93.30 HRS
95.00 HRS



(ET!
(ET)
(ET)
(ET1
G E :
(ET)
JIETJ_
(ET)
(ET)
(£T)
AVERAGE:
_81.CO_HRS_IEIJ 	
96.00 HRS (ET)
A V E R A

67.00 HRS
95. CO HRS
A V £ R A

83.20 HRS
65.20 HRS
S3. CD hRS
9C.10 HSS
94. CD H?.S
96. CO HRS
A V E R A

31.00 HRS
8S. CO HRS
97. CO HRS_
T 0 T A
RAT

31.00 HRS
97.00 HRS
T 3 T A
RAT

SI. CO hi»S
=9. CO HRS
97. CO HRS
G E :

(ST)
(ET)
G E :

(ET)
(ET)
JET)
JET)
!ET!
(ET)
G E :

i£T)
1ST)
(ET)
L :
E :

(ET)
!cT)
..t__- 	
E :

!ET)
(ET)
(ET)
ERATING PERICC:


S 0 2 SCR
S02 CCNC INLET FLLE G.'S
S02 CCNC INLET FLLE Gi S
S02 CCNC INLET FLUE G/S
S02 CCNC INLET FLLE G< S
SC2 CCNC INLET FLUE G/S
S02 CCNC CUTLET FLL'E i. AS
SC2 CCNC CUTLET FLLE CAS
SC2 CCNC CUTLET FLUE CAS
S02 CCNC CUTLET FLLE (-AS
SC2 CCNC CUTLET FLUE (.AS
S02 CCNC CUTLET FLUE Ci.'i
H20 CCNC INLET FLUE GiS
H20 CCNC INLET FLLE G.'S
H20 CCNC INLET FLUE G^S

CRIFICE PRESSURE CRC?
CRIFICE PRESSURE DSC?
CRIFICE PRESSURE ORO°

CRIFICE TEMPERATURE
ORIFICE TEMPERATURE
CSIF1CE TEMPERATURE
GRIFICc TEf-'FERATUSE
GRIF1CE TEFFERAYLRc
CRIFICE TEMPERATURE
GRIFICE TE!*PERATLRE

WEIGHT CYCLCNE DLST
V.EIGHT CYCLC.NE CLST
WEIGHT CYCLCNE DUST
WEIGHT CYCLCNE CUST
WEIGHT CYCLCNE CUST

VsEIGHT CCLLECTOR DUST
fcElGHT CCLLECTCP. DLST
WEIGHT COLLECTOR DUST
hEIGHT CCLLECTCR DUST

WEIGHT CAKSCN '.iOEPAGS
UEiGHT CARSCN WEEPAG6
WEIGHT CAR8CN WEEPAGE
'


B E R
(GS-
(GS-
(GS-
!GS-
(GS-
(GS-
(GS-
!GS-
IGS-
-;GS-
(GS-
(GS-
CGS-
:GS-

(CP-
iCP-
IOP-

(TL-
UL-
(TL-
iTL-


12)
120
12!



,•
.CO HRS LENGTH OF PERIOD: 15.00 HRS '•:




/ Y10U,T) -
/ VICtl.T) =
/ YiC(ltT) =
/ YlO(l.T) =
/ AY10A =
/ Y1651.T) =
/ Y16(1,T) =
/ Y16I1.T) =
/ Yl&tl.T) =
/ Y16U.T) =
/ AY16A =
/ YiOtl.Tl =
/ Y10(4,T) =
/ AY10C =

/ r P i o i T i -
/ CP10(T! =
/ ADP10 =

/ TL101T) =
/ TLIO(T) =
/ TLlOiT) =
/ TLIO(T) =
/ TLIO(T) =
/ TLIO(T) »
/ ATL1C =

/ C01KT) =
/ C01KT) =
/ CD1KT) =
/ «D11
/ RCil =

/ CD121T) =
/ CD12IT) =
/ k-012 =
/ R012 =

/ CV.121T) =
/ CW127
:i
u
*
.-.

-------
i
i
i
;=:
.4
!.
i t
>'
1
;'
-;
V


12:
20:
4:


12:
20:
4:





15 HRS
15 HRS
.3,5 HRS


15 HRS
15 HRS
15 HRS




T
si.cc
as. co
S7.CO
A v e

81. CO
as. co
97. CO
A V £



0 T A L :
R i T E t
HRS
rRS
3 A
HRS~
HRS
HRS
S A



1£T!
1£T!
;ET)
G E :

(ET)
1ST)
(ET)
G £ :



WEIGHT C4RBCX WEEPAGr
ft
*»


S
•w
%
«



TCT S
TCT S
TOT S
TCT S

TOT S
TOT S
TCT S
TCT S



C\
CN
r\
CN-
ni 	 	
CN
CN
CN
CN



CYCLCNE C.JT
CYCLCNE DUiT
CYCLONE CwJT

CCLtECTOR CL5.T
CCLLECTCR 1U5T
CCLLECTOR :U5T
CCLLECTCS :LST



ICh-
JCW-
! D-
I C-
{ C-
( D-

( D-
< 0-
; o-
( .c-



12) /
12) /
11) /
111 /
11 ; /
in /
12) /
12) /
12) /
12) /



WCK12 =
RCH2 =
011(1
C1H1
011(1
T « _
t ' I ~
,T) =
,TI =
A011A =
012(1
C12U
012(1
AD




t T) =
,T! =
»T) =
' 24 »



4/23/74 PAGE 2 ]
1
0.125 IS CUST ' j
C.008 L3 CUST/HR |
j
6.740
7.120
7.300
7.053

6.740
7.120
7.500
7.120



? UEIGHT)
S (V.EIGHT)
? (XEIGHT)
1 UEIGHT)

S (VtEIC-hT)
S (WEIGHT)
J (V.EIGHT)
* (hEIGHTJ





-•:

.-':
•><
••:'
;.,•
i'*
K
                                                                                                                                                                                            - -l'3,
u>
o
VO

-------
4/23/7*
            PAGE

1,-
';i — —
;;'
.a
•1

1 "i
it
••-
:l
[)
5=
is
f
i";
D
t!
s*
H

G
D
Q
t-
k

c
IJ
q .
1 • ™ • ii— •
j

j 	

! 	
, 	
S*
P! 	 	
&" DIA CARBON PRECONCITICNER
	 .13:15 HRS .87.00 HRS SET) S TOT S ON INLET CARBCf. 1CS-301) / ZHOU1.T) =
17:15 l-?,5 S6.CO H*S !ET! < TOT S CN INLET CA3EC.. (CS-2I1! / Z'Cl'ltT) »
12:15 t-RS S.CO r'.S !£T) ? TOT S CN I .'.'LET CA3:C.. {CS-iClJ / 2301(i,T) =
— » 	 I.:.l5 HR.S 9A.CO H^S 1ST) ? TCT S CN INL^ET C/SRSC. -ICS-3C1) / Z2CK1.T) =
	 A V F R A G F : * THT' S CN IMET CiRFr;, (CS-301) / iVZ301* =
13:15 HSS 8J.cn >-«<; IFTJ J H20 ON INLET CARECN ICS-3C1) / Z301I2.T) =
17:15 MRS 36. CO MS (ET) S H20 ON INLET C4RBCN 5CS-2C1) / Z3CK2.T) «
21:15 KRS 9C.CO i^SS (ET) S r20 ON INLET CARSCN ' (CS-301 ) / 23C1!2,T) =
iv?R4GE: 5 H20 CN INLET CiREON ICS-3015 / AZ3C1E =

12:15 HRS 31. CO t-K3 t£T) xSIGHT CYCLCNE OUST « C-3C1) / CD30KT) =
4:15 HRS 97. CO HRS (ET) WEIGHT CYCLCNE OUST < D-301! / CD30KT) =
T C T S L : WEIGHT CYCLCNE CUST { C-2C1 ) / WD3C1 =
RATE: WEIGHT CYCLCNE CCST < c-3ci> / PDSOI =
12:15 HRS 81. CO HRS (ET) % TOT S CN CYCLCNE CLS" 1 0-3CI) / C30K1.T) =
3:15 HRS 96. CO HRS ( ET ! t TOT S ON CYCLCNE DL'SV I C-3011 / D1O1!1.T) =
AVERAGE: * TOT S CN CYCLCNE OUS'" 1 D-301) / AD301A =









.
*





•








8.560 S (WEIGHT)
8.640 1 (WEIGHT)
8.560 % (WEIGHT)
B-640 t (ViEIGHTJ
8.605 % (WEIGHT)
8.800 * (WEIGHT)
6.400 S (WEIGHT!
7.500 ? (WEIGHT)
7.567 5 (WEIGHT)

0.0 LE CUST
0.0 LB CUST
0.0 L6 CUST
0-0 IS CUST/HR
0.0 * (WEIGHT)
0.0 t (WEIGHT)
0.0 S (WEIGHT)

























. 1
j

!
t.
'.3
'..<
^
'-$
"«i
'-1

r
t=
ts
u
y
"*
s!
-«'
33,
3

u
b*
~ !
3-"
'^
^
IJ
.S
^
k^
d'
ia
_•;
t-
',4


-------
                                                                                                                 4/23/74
                                                                                                                            "PAGE
c:
                                                            U L F li R
                                                                               E R A T  C  R
L
I' I
ir
':
,:'

1:
(f :
l;
U 	

|=; — . 	
f^
!:»

w
d-
.

j:-
M
y
a-
H
b*:
ES
u1
H
Ly
!i'
:•=
!•=
H
?*
L
i.-!
U'
r:
U
!r]
i.'
i.t
17:50
0:15
6:15

16:15
22:50
4:26
17:50
C- 1 C
5:15
16:15
35. «A
4:26

17:50
0--15
6: 15


16:15
22:50
4:26


17: 50
0:15
6:15
'
2:15
22:50
4:26
17:50
0:15
6:15
12:15
3:15


13:15
17:15
21: 15
1:15


13:15
17:15
MRS
HRS
HRS

HRS
HRS
HRS
HRS
us c
HRS
HRS
HRS

HRS
HRS
_H».S


HRS
H'cS
.HRS.


HRS
HRS
hRS

HRS
HRS
nRS
HRS
..HRS
HRS
HRS
HRS


h.RS
HRS
hRS
HRS


HRS
HRS
36.60
93.0:
9-S.CC
* V *•

S5.CO
91.6.0
97. 2C
A V E
S6.60
9"* *" *^

A V =
35.00
97.20
A V E
35.60
93.00
99.00
A V E

85.00
91.60
97.2?
A V E

86.60
93.00
99.00
A V E

95. CO
91.60
57.20
A V E
36.60
93. CO
99. CO
A V E
81. CO
96.00
A V E

32.00
66.00
SC.CO
94. CO
A V E

62. CO
86. CO
HRS
HRS
HSS
R A

HRS
HRS
HRS
R A
HRS_
" Q C
HP.S
R i
HRS
• O C
"hRS~
R A
HP.S
HfiS
R A

HRS
HP.S
HRS
R A

HRS
HRS
HRS
R A

-HRS
HRS
hRS
R A
HRS
HRS
HP.S
R A
HRS
HRS
R A

HP.S
HRS
HRS
HRS
R A

HRS
nRS
(ET)
IET)
SET)
G E :

(ET)
(ET)
(ET)
G E :
'. ET)
(ET)
G e -.
(ET)
(ET)
G £ :
(HT>
(ET)
(ET)
G E :

(ET)
(ET)
•£T)
G E :

(ET)
(ET)
(ET)
G E :

1ST!
JET)
(ST)
G E :
(ET)
(ET)
IET)
G E :
(ET)
IET)
G E :

(ET)
(ET)
(ET)
(ETI
G E :

i£T)
SC2 CCNC CUTLET GAS
S02 CCNC CUTLET GAS
$02 CCNC CUTLET GAS
$02 CCNC CUTLET GAS

H2S CCKC [NLF.T GAS
H2S CCNC INLET GAS
H2S CCNC INLET GAS
t-.2S CCNC INLET GAS
h2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CC,\C CUTLET GAS
H2 CON'C INLET GAS
HZ CUNC INLEf GAS
h2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CCNC CUTLET CiS
H2 Cuf.C CUTLET GAS
H2 CONC CUTLET GAS
h2 CONC CUTLET GAS

H20 CCNC INLET GAS
H20 CCNC INLET GiS
H2C CCNC IM£T G-'b
H20 CCNC INLET GAS

H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
h20 CCN'C CUTLET GAS
H20 CCNC CUTLET GAS

N2 C3NC INLET GAS
,N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CCNC CUTLET GAS
N2 CCNC CUTLET GAS
N2 CONC CUTL.ET GAS
N2 CONC CUTLET GAS
N2 INlcT VCL FLCh R S~'E
N'2 INLET VCL FLOK RITE
N2 INLET VCL FLCVs RAVE

S TCT S CN INLET C«^:CN
1 TCT S CN INLET CSV:CN
S TCT S CN INLET Cfi'ViCN
S TCT S CN INLET CA 5;.'GN
% TCT S CN1 INLET Ci\ JCN

Z TCT S CN CUTLET C J '.BCK
3 TCT s CN C-JVLET c* ;ECN
(GS-206)
:GS-206!
!GS-2C6)
IC-S-2C6!

iGS-200 i
5GS-20C)
iGS-200)
JC-S-iCO)
JGS-2C6)
f f ^ T* ' \
\ G5 ^C o )
iGS-2C6)
SGS-2C6)
(GS-2001
r f* c "5 P f* i
5GS-2C03
!GS-2CC!
iGS-2C6)
!CS-2C6!
(GS-206)
(GS-206)

(GS-2CO)
'GS-2C3J
(GS-2CO)

5GS-206)
1 -:GS-2C6)
(GS-206)
!GS-2Cfc)

fGS-200)
(C-S-2CO)
(GS-2CO)
JGS-2CC)
4GS-20S)
(GS-206)
(GS-2C6)
(GS-206 !
! G-2CO!
< G-2CC)
! G-2CO)

iCS-302)
(CS-3C2)
(CS-302)
JCS-302 )
' (CS-3C2)

;CS-2CC)
:cs-2eo>
/
/
/

/
/
/

/
/

/
/
/
/

'/
t

/
'

/
/
/
/
/
/
/
/
/

't
/
/

/
Y206(1,T). =
Y2C6tl,T) «
Y206I1TT) =
AV206A =

Y200J2.T) =
Y200!2,T! »
Y2CC!2,T) =
AY200S =
Y20il2,T) =
Y2C6I2.T) =
AY206E =
Y200(3,T) =
V OP f\ f Ti T \
Y200!3,T> =
AY200C =
Y206!3,T) =
Y2C6(3,T) =
V206!3,T) =
AY206C =

Y2°Ci4'T! =
AY2CCC =

Y206(4,Ti =
Y206!4,T) =
Y2C6(4,T) =
AY2C6C >

Y200I5.T) =
Y200I5.T) =
Y2CO(5,T) =
AY20CE =
Y2C6J5.T) =
Y206!5,T) =
Y2C6!5,T! =
AY206E =
G2CC15,T) =
620015,7) =
AG200E =

Z302(1»T) =
Z302I1.T) =
Z302!1,T) =
Z302tl,T! =
AZ302A «

1200 il,T) -
2200(1,7) =
1.500
1.530
1.470
1.500

27.200
26.000
26.300
26.667
0.0
C/i
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0

21.200
19. SCO
2C.OOO
2C.333

53.200
51.300
50.500
51.667

51.100
53.9CC
52.600
52.600
45.000
46.7CO
47.700
46.467
121. COO
321.000
121.000

8.560
8.5SO
8.640
8.605

19.800
19.600
? (VCLUHE)
t (VCLUME) !i
? (VCLUCE) S
? (VCLUKS) |i
',
? (VCLUME) j.
J (VCLUHE)
S (VCLUXE) >
? CVCLUKE) ,
t
% 1 VCLUME)
? ( VCLUXE i •:
? (VCLUHE) .:
? (VCLUKE) :..
S (VCLUKe) |:.
S (VCLUHE)
S. (VCLUKE) !?
S (VCLUME) !:
? C/CLU.ME) T
S (VCLU.VE) ir
L
3 (VCLUME) -.
S (VCLUVc) (-.
?! VCLUME; ~
w
S (VCLUME) »
? [VCLUHE! j,
? (VCLUME) i.
? (VCLUKE) '•-
:
? (VCLUME) '„
S (VCLUNE) r-
S (VCLUME) ;-.
S (VCLUME) '?
ir
S (VCLUKE) ^
? (VCLUHE) ;
% tVCUJ^E) ;..
% (VCLUfE)
CFK (7C CSG F) [
CFH (7C CEG F)
CFH (70 CEG F) I
1
S (h EIGHT)
? ("EIGHT)
T (HEIGHT)
1 (V.F.IGHT)
S (UEICHT)

S tfcEIGHT)
Z IWEIGHT) „

-------
                                                                                                                        PAGE
      C|
00
1
i

r

•
;
•>
.•*
*.
L,
c-
"i.

•*
::.
~
-,
-..
21:
is
13:
17:
21:


13:
17:
71:
1:

.
13:
17:
21:
15






15 HRS
15 HRS
15 HRS
15 HRS
15 HRS


15 HRS
15 HRS
15 HRS
15 HRS


15 HRS
15 HR S
.15. HRS. .
15 HRS


•



•9C.CC
S'..CO
A V c
8 2. CO
_ 36. CO
9C.CO
A V E

82. CC
H6.CO
-.5C. CO..
94. CO
A V E

32. CO
S6.CC
<=C.CO
SA.CO
A V E





HRS
H3S
R A
~RS
HRS
R A

HRS
HRS
HMS
R A

HRS
HRS
H-.S
HRS
R A





(ET) 3
icT) 4
G E : ?
iET! ^
!FT) \
IET) S
G E : 3

(ET)
1ET)
(ET)
G E :

(ET)
(ET!
;ET>
(ET)
G E :





E TOT S ON CUTLET CAi
(WEIGHT)
;
(WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT)
(WEIGHT) s:
rr
7
_
_
z.
      O

-------
1
I
f'i 19:15
i*i 1: 2
w
'«! 14: 38
21:15
3: 2
:*•
•=i 5:15
''' ' 19:15
'•*' l: 2
W
U 14:3£
\* 3: 2
'*'
'?'. 14:3E
i-' 21:15
!=* 3:2

Ij
'=> 14:33
;- . 21:45
- 3: 2

t . 	 	 	
W 12:15
•f'= 3:15
Ji

;>: • A: 15

U! 12:15
Id 4:15

i — — — 	 	 —
13:15
-:• 17:15
U 21:15
HRS
HRS
HRS

hRS
HRS
HRS
HR.S
HRS
HRS
HRS
HRS
HRS

HRS
HRS
H*S_

HRS
HRS
HRS


HRS
MRS
HRS
KRS

HRS
HRS


HRS
H'RS
HRS
y 1:15 HRS


IJ 12:15 HRS
3:15 H?S


81. SO
88.00
93.50
A V' E

83.40
9C.CO
95.60
A V E
ais.cc
83.00
93.80
A V E
83.40
9C.CO
95. BO
A V E
83.40
9C.CO
95.30
A V E

63.40
9C. 50
A V £

81. CO
96. CO
A V E
31. CO
97. CO
HRS
HRS
HRS
R A

HRS
HRS
HRS"
R A
HRS
HHS
HRS"
R A
HRS
HRS
HRS
R A
H?.S
HRS
HSS
R A

HRS
HRS
IfC*_
HRS
HRS
R A
HRS
HRS
TOT
81. CO
97. CO
T

82.00
34. CO
sc.cc
94. CO
A V E
51. CO
i V E
R A
HRS
"HR s
0 T
R . r.
H.5S
HRS
HRS
3 A
K
(ET)
(ET)
(£T|
G E :

iET)
!ET)
!ET!
G c :
(ET)
(ET)
(ET)
G E :
(ET)
(ET)
1ST)
G E :
!ET)
,
(iET!
G E :

(ET)
IET)
G E :
!ET!
(ETJ
A L :
T E :
!£T)
(ET)
A L :
T E :
'. ET)
(£T)
(ETJ
G E :
rRS ;CT)
H s T, '. : " I
f< .'
.5..E..--
2S GENE.RATCR/JUtFLR
H2 CONC INLET GAS IGS-1CO)
H2 CONC INLET GAS
H2 CGNC INLET GAS
H2 CCNC INLET CA<
,
H2 CON'C CUTLET GAS
H2 CCKC CUTLET GAS
H2 CCNC CUTLET CAS
H2 CONC CUTLET GAS
N2 CGNC INLET GAS
N2 CDNC INLET GAS
N2 CCNC INLET GAS
N2 CCf.C INLET GAS
N2 CCNC CUTLET GAS
N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CC,\C CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS

H20 CCSC CUTLET GAS
H2Q CCNC CUTLET GAS
H20 CC.-.C CUTLET GAS
H20 CCftC CUTLET GAS

N2 INLET VCL FLO* RATE
>N2 INLET VCL FLO* RAT!
N2 INLET VCL FLC',1 RAT!
HEIGHT CYCLCNc CUST
HEIGHT CYCLCN'E CUST
HEIGHT CYCLCNE OLST
VvEIGHT. CYCLCriE CUST
WEIGHT FILTER CUST
WEIGHT FILTER CUST
HEIGHT FILTES CLST
WEIGHT FILTER CUST
g TCT S C\ CVCLC.NE Z'^Z~
% TOT S ON CVCLCi-.c CL1- '.'
% TOT s CN CYCLCNE o-_. T
% TOT S CN CYCLCNE C', 'l
% TOT S CN CYCLCNS D: ">
'.. TOT J -0, FtLTCR DUS
% TOT S CN FILTES G'.S
?> TOT S C\ FILT5R CtSi
5GS-1CO)
(GS-1CO!
(GS-1CC '

(Gs-ica:
iGs-ice;
tcs-ica)
{GS-iCS}
(GS-1CC!
!GS-1CO>
(GS-1CO)
5GS-1CO)
(GS-1C3)
(GS-10S)
CGS-LOS)
5GS-1C8)
'GS-1C£ )
CGS-108)
iGS-100)

iGS-103)
CGS-1C3)
CGS-1C6)
iGS-lCc )

! G-1CO)
I G-1CO)
( G-10L-)
i C-1C1)
\ O-iOl)
J C-101)
( C-101 !
( D-IC2)
( C-1C2)
,' D-1C2I
{ C-1C2)
j c-ic:)
( C-iCl)
( C-1C1!
; o-ici)
; C-1C2)
( 'J-1C2!
', C-1C21
STRIPPER
/ Y10Qt3,T) =
/ VlOOlStT) »
/ YIOOI3.T ) =
/ AYIOCC =

/ Y108(3tT) «
' Y108(3,T) -
/ V1C6O.T) =
/ AYicec =
/ Y100!5fT) =
/ YiCC(5,T) =
/ Y1CO(5. T) =
/ AYiOOE =
/ Y103(5,T) -
/ Y1C3J5.T) =
/ Y10315.T) =
/ AY106E =
/ Y1CS!2»T! =
/ Y108(2,TI =
/ Y103(2fT) =
/ AY10SS =

/ Y!Cc!4, T) •*
1 ViOSCltT) =
/ AY102C =

/ G100!£,T) =
/ G100S5.T! =
/ AG100E =
/ CCiCliT) =
/ CDlOliT! =
/ Vi 0 i 0 1 =
/ RC101 =
/ C01021T) =
/ CD1C2U) =
/ WC102 =
/ RD1C2 »
/ D10i;i,T! =
/ ClOliltT) =
/ ClCKl.T) =
/ AD101A =
/ DlC2(ltT) =
/ C 1 C ; ! I , T ) =
/ A01Q2A =
50
51
50
5C

0
0
4/23/
.700 %
.200
.600
.533
.0 ~
.0
c.o
0.0
49
48
49
49
50
52
53
52
29
23
28
23

19
19
17
18

121
121
121
0
C
c
c
c
0
0
c
2
4
4
4
0
0
0
.300
.800
.400
.167
. 500
.200"
.300 ~
.000
.600
.100
.600
.767
;so.o~
.300
.800
.867

.000
.000
• CCO
.0
.0
.0
.0
.0
.c
.0
.0
.coo
.920
.200
.030
.050
.0
.0
.0
9
*
O
i«
«
*
S
?
I'
z
%
%
a
*e
s~
*f
^
%
t
CF
CF
CF
L3
L6
L3
ie
LS
LB
L8
LE
f
%
n
*
x
74, PAGE 6
t VCLUME) j
(VCLUME) ;•'
(VCLU.'i;! |;
(VCLUME) is
•
(VCLUXE) i
JVCLUHEJ
(VCLU.VE) :.•
(VCL'JKE) ;•
! VCLUME) sa
(VCLUXE) 'i.
( VCLUME i -.=
(VCLL'ME! >
(VCLUME) -5
(VCLUME) !•,
(VCLUME) .--,
(VCLUME) -«
( VCL'JJ'-c) ::
(VCLUKE) :,
(VCLUWE) n
-i
(VCLUVE) '-<
(VCLUME1 '-.i
(VCLUNE) s,'
T>
H (7C DEC F) »
h !7C CEG F)
H (7C CE3 F) ;.,
CUST ^
CUST '-i
CUST W
CUST /HP ;J
CUST .',*
CUST ^
CUST
CUST/HR ,i
(WEIGHT) J
(VEIGHT) L,:
("EIGHT) J
('.EIGHT) ^
(V.EIGMT) '.^
('/.EIGHT) ^
(-EIGHT)
(V, EIGHT) ,,

-------
                                                                                                                          4/23/74
                                                                                                                                       PAGE
U)
1
1
1
!
!
> 	
i3: : •

'i:
!•:
• >• -
!'•
1S
<'-•
;*
-.*
* 9
-»'
r".
ja
ti
t.'
r :
-i
k .
bai

j"*
: i 	
M

s*

r
r .
U4
n 	
»', 	
CARBON INVE
13:15 HRS a?-1"?; <-a S RESIDUAL S CM CARBCN
AVERAGE-: X RESICUiL S CM C'ARECH

17: 15 HRS 86. CO rRS IET) $ SSSIC'vAL H2C CN CAREt.N
21:15 HRS 9C.OO "-PS JET) 3 RESIDUAL H2C CN CiREtN
1:15 HRS 94. CO r?S (ET) % RESIDUAL H2C CN CASEIN
AVERAGE: S RESIDUAL H20 ON CARfit N

12:15 HRS 31.00 r'S JET) CAR9Cfc RECYCLE R4TF
3:15 HRS 96. CO >-RS !ET) CAR2CN RECYCLE RATE
AVERAGE : CAR20N RECYCLE RATE

SULFUR CON

11:15 HRS 8C.CO HRS (ET) xSIGHT SULFUR CQLLECTE!:
13:33 HRS 82.40 HRS (ET) HEIGHT SULFUR CCLLECTEi:
IS: 15 HRS 87. CC HRS (ETI WEIGHT SULFUR CCLLECTE!'
TOTAL: WEIGHT SULFUR CCLLECTE;:
RATE: WEIGHT SULFUR CCLLECTEi:







•





.
N T- C R Y H
{CS- 90) /
(cs- 9c; /
' -:cs- <:c> /
{CS- 9CJ /
tCS- 90) /

%L S 90 ) /
!CS- 9C! /
1CS- 9C) /
(CS- 90) /
(CS- 90) /

{ C- 90) /
', C- 90) /

CENSER

! S-4C1) /
! S--401! /
( S-401) /
I S-4C1) /














! C P ? E R
29C!1,T) »
Z9C(1,T) =
A29CA =

Z90 ( Z» i ) =
Z90(2,T) =
290(2, T) =
Z90(2tT) =
AZ9CS =

C90U.T) =
C<50(1,T; =
AC9CA =



S4CKT) =
S40KT) =
S4CUT) =
WS4CI =
RS4C1 *














4.000 ;
3.920 ?
4.200 ?
4.080 ?
4.050 ?
2 "3 ^f\ 1
• Z30 %
2.230 ?
2.230 %
2.230 ?
2.230 S

31.000 LB
31. COO LB
31.000 LB



0.0 LB
4.200 L3
8.000 IB
12.200 LB
1.743 LB














(••EIGHT)
UEIGHT)
(V.EIGHT)
(V.EIGHT)
(ViEIGbT)

(VsEIGHT)
(WEIGHT)
(HEIGHT)
(WEIGHT)

I'AT'L/HR
MAT'L/HR
KAT'L/H'R



SULFUR
SULFUR
SULFUR
SULrUS
SULFUR/HR














j
1
3-
I.I
Is!
i
(
I't
k>
.*,
,'
-,'
1,

.,
— • i
33
-.'
j:
-,
,.
'~i
r?
~_-

-;
^
:
-j
-or
-
       ^<£






       hr

-------
Ui
!
!
.1
:«:
'.!
's!
.'
»,
?a
,J
STATUS REPCST CF OPERATING
OPERATING PcSiCO:
v CATE: 4/23/74 TIKE OP RE
CCKCITICNS FCR
CCRC: 12:15 H
CATE: 4/24/74 TIME OF RECCRC: 0:' C h

PRCCESS cLAPSEC TIfE CF PERIOD
-
: ..START 81
|
INTEGRATED CPERATICN CF S02 RECCV5RY PROCESS i
: f
;!S TC 24: 0 HRS •'--!
'•IS TC 3:15 HRS ' ,«i

.CC HRS / £NE 96.CC rRS LENGTH GF PERIOD: 15.00 HRS ;.
SUMMARY CF INTEGRATED PRCCESS PERFORMANCE: . >!

1. S02 REMOVAL

PRS02 =
•,
93.87 Z (ACTUAL! . ?0.0 * (GCAL) '.«
H • • ':
[J
*-
-
i
ii
loi
it
J
f*

H
y

0*
W
3*-
a-
y
u
TI 	
• '
i ^

2. H2S UTILIZATION
3. ACiO CCNVERSIC.N I TC SULFUS)

4. H2 UTILIZATION I TO K2S)

5. SULFUR RECOVERY
6. H2 LTILIZATICN 4" tMT

7. RcSICUAL SULFUR ON CARSCN
8. CAR80N RECYCLE RATE (D6!
9. ACIO LCACING INLET CtRECK S" UNIT

10. H01STURE CCNTEttT l^aET CARSCN 6" UNIT
11. ACID LCACING IMLET CARBON S" UMT
12, C.CISTL'RE CCNTENT INLET CARBCN 8" UNIT

13. TOTiL ACIC CCNVERTtD S" U.NIT
14. SULFLR CC.\VERSIO\' iTC H2S)
15.  »
55.73 % (ACTUAL; ??.c ? (GCALJ -i
»l
7C.46 % (ACTUAL) 50.0 ? (GCAL) -,
\t
EC. 91 S (ACTUAL) 1CC.C 3 (GCAL) OF SORSEC SC2
27.22 S (ACTUAL) 25. C S ( GCAL ) OF STRIPPED SULFUR -A
ICC. CO 3 ri
•^
C.C432 LB S/L8 C :<
25.053 LS C(DE)/HR ;,;
C.2309 L3 ACIC/LB C ^
^
0.1C43 LB I-2C/L2 C K
C.2309 LB ACIO/LB C r.
C.1043 L6 H2C/LE C -^
:s
36.88 S . *
= 6.66 % '.
2:3.97 ?
_.
,;
.«
TKlTliTCf, p^rrsrua's TO TAKE SC2 CUTLET
L.J 	 SAMPLE FROM 18" UNIT UNDER POSITIVE PRESSURE


-------
                                                                                                                        4/23/74




                                      STATUS R5?CRT CF CPERATING CCNCITICNS FCR 1MEGRATEO OPERATIC* CF  S02  RECOVERY  PROCESS
                                                                                                                                    PAGE   9
Co
;'
••

••
« :.
t
" J


Q
..,

!'*'
l" ;
n
r*
5*

U,
H"
*i
LJ
a
r*

OPERATING PERIOD:
CATC: i/23/74
CATE: 4/24/74

PRCCESS 5LA=SEC
SULFUR CATERIAL BAL*N



! N
INLET
INLET

CUT
CUTLET
CLTLET
TIME OF RECCRC: 12:15 HRS TO 24: 0 s~
S




TIKE CF RECCRC: 0: 0 SfS TO 3:15 HSS

Tiy= CF PERIOD:
CE (USING PROCESS



GAS AS S02
T C T A L IN

GAS AS SC2
CA5BCN
CYCLCNE CUST
CCLLECTCR OUST
C4RSCN
T


I N
INLET
CUT 	
CUTLET
SEEPAGE
C T A J. OUT
6" D I A C


CARBON
T C T A L IN

CARSCN
CYCLCNE CUST
•:#
r •. 	
l .;
T


C T A L OUT
S U


START := .
H2S):


S 0 2
( G -
( C—
: ( R v-

( G-
( C-
I D-
{ 3-
(Ck-
: IRV-
ARSON



, r ; j^



s : R
13)
\\\

13)
12!
11)
12)
12)
1C)
P R


1 C- 12)
: [RV-.-JCC)

( C-

2 CD
( c-;tci)
: (RV-
L F U R

:;cci
G E


RS / END



3 £ R
/ SG10A =
/ 3C11A =
/ sno =

/ BC-13,2 =
/ BDilA =
/ ED12A =
/ BCW12A =
/ S010 =
E C C N D


/ BC12* =
/ SI3CO =

/ BC2CIA =
/ 8 D 30 14 =
/ S03CC =
N E R A T C


95.CO




2
1
3

C
•3
C
C

I-RS




.2949
.'2555
.5504
. 1407
.4462
-C121
.C
C.CC09
3.5999
I T I


3

3
C
2
R

C N


.44i2

.4462
.C
.-,4£,:








LB
"LB
LS
LS
LB
LH
" LS
LB
E R

••
LB
Lc

_LB
LB



LENGTH CF PERICC: 15.00 HRS




SL'LFUR/(-R
SULFUR/f-R

S'JLFUR/HR
SULFUS/J-R
SLLFUR/h?,
S'JLFUR/S-R
SULFDR/1-R
SULFUR /i-.R



SULFUR/i-R
SULFUR/hR

SLJLFUR/I-R
SULFUR/f-R
Sl-LrjR/HR


.
,
t
;

-:
<
	 *
..
':
_
a
:4
f
rr
-s
;,
3
M
-,
;,-
-
^.

U I N -=
: J
j i
0
1 	


J-
i.,
I\LET
INLET
INLET


CUT
CUTLET
CUTLET
t
GAS IS H2S iCYL!
GAS AS H2S (PRCC)
CARBON
T C T A L IN


GAS AS H2S
GAS AS S02
CAR6CN
C T A L OUT
( G-
( G-
( C-
: 

•:C5)
;2co
/ EG2C13 =
/ BG232R =
/ SI2CC =


/ 5G2052 =
/ BG20Si =
/ BC2G2A =
/ S02CO =
C
5
3
3


0
C
7
7
.0
.5491
.4462
.9953

.0
-322S
.6591
.9829
LE
LS
_Lc
L c
LB
13
LE
LE
SULFLIR/HR
SULFUR/hR
S'JLFUR/t-R
SUL.FUR/I-R


SUL?'JS/HS
Si..LFUR/1-R
S'-LFUR/f-R
SULFUR/i-R
'1
^
.-
.-.
.-.
"

-------
                                                                                                                                     PAGE  10
                                                    H 2 S
                                                             G £ N E R & T CR/SULFUR
                                                                                                 S  T  R  I  P  P
                                      I N
LO
INLET CAR3GN

I-
I*1

-3
J-
::
|-:
**.
J"»

3-'
'->
03
^


CUT
CUTLET
CUTLET
CUTLET
CYCLCNE
FILTER
T


I N
•NLET G
T C T


CAS3CM
GAS -AS
GAS AS
DUST ~
CUST
C T A
C


AS 13"
INLET GAS 8"
CUT
OUTLET
CYCLCNE

GAS 13
CUST
A L I


1-2S
S


L C U
VESA


UNIT AS
UK IT AS
T Q T

N :





T :
L L


SC2
CYL H2S
A L

" UNIT AS SC2
18" UMT

= COLUECTCK CUST IB" 'oMT
» CAR2CN '*EEFACE 16" UNIT
'=• CYCLCNE CUST 6" UMT
~r
'-f
y,
CUTLET
CUTLET
OUTLET
GAS 8"
UNIT AS
GAS 3" UNIT AS
GAS 4" UNIT AS
'••?. CUTIST G^S 4" UK IT AS
M CYCLCNE CUST 4" UNIT
= FiLTES CUST 4" UNIT
5»(


T C T A
H2S
SC2
H2S
S
L S
! C-2C2)
, (R'v-UC!
rf

< C-1C3)
( G-1C4)
( S-IC4)
( c-i: i)
( C-IC2)

( r-iC2i
U L F L R
/ 5TC2C2A =
/ SHOO .=
.

/ EC103A =
/ BG1C4S =
/ BD101A =
/ 8C102A =
/ SOiCC =
R 3 A I t


/ 8G10A «
/ DC201B =
R IN:


3«i.3A -
/ 6011 A =
/ £012 A =
/ 8CK12* =
/ 30301 A =
/ DG205S =
/ 3G205A =
/ SS10AB =
/ EGIOA3 =
/ E0102A =
GUT:
7.
7.


1.
5.
V *
C.
3.
i N C


2.
C.
2.

0.
0.
C.
c.
c.
c.
c.
c.
^ •
c.
0.
2.
65<31
6551
2555
EAS1
0
C
P

2949"
0
2SA9
1407"
012T
0
CCC5
2
n
32.38
C
7A29
C
/>
2.?0_4_
L:
LE
L 3
LB
L £
L3
LE


L8
LE
LS
L3
LE
LS
LE
LE
LB
L2
LS
L2
L2
LS
S'JLFUa/i-S
SULFUR/hR


SU'LFUR/hR
SULFUR /?"R
S'Ji.FUR/1-K
SULFUR /HR
SULFt;R/^S



SULFua/hR
SULFUR/V--R

SULFUR/J-R
SULrUR/HR
SULFUR/I-R
SULFUR/HR
SULFUP/f-R
SU-LFUR/--R
SULFua/hF.
SULFL S/I-R
SULFUR/i-R
SULFUR/hR
SULFu'R/t-R

;«;
!:i

!'-
•I'.
.jj
.-;
•s!
•3
' t
'•*
H


*<
73
rf
?a
s«
-'*
,;
7»
;3
'3
_l

-------
                                                                                                                      4/23/74
                                                                                                                                  PAGE 11
                           HYQRCGEN MATERIAL  Bi
u>
I-1
oo

IN.
TKIPT
T OL' f C T
INLET
I\LET
INLET
CUT
CUTLET
OUTLET
OUTLET
OUTLET
T


GAS AS.
r • c * c
G.'.S AS
GAS AS
CAR3CN
T C T
GAS AS
GAS AS
GAS AS
CARBCIM
C T A
SDL

H2
iJ 5 C f f" VI \
•r2S (PRCC)
H20
A L IN:
r2
H2S

L OUT:
FUR G = N

( G-2C3) /
!
HYCRCGE^/l-R :'|
HYCRCGEN/I-R '.|
hYCRCGEN/HR '.
HYCRCGEN/hR H,
HYCP.CGEM/HR <;
HYCRCGSN/hR •»'
HYCRCGEN/HR 1:-
lj

I N
INLET
INLET
1
I
i CUT
H 2 S

GAS AS
CASSCN
T C T
1 CUTLET GAS AS
! CUTLET
.OUTLET
! T
GAS AS
GAS AS
C T A
G E N E R

H2

A L IN:
H2
I-2S
H20
L GUT:
ATCS/SUL

! G-K3) /
( C-2C2) /
(Rv-lfC) /
( G-1C4) /
! G-114) /
! G-H4J /
(RV-:tCi /
FUR

BG103C =
EC202H =
HUGO =
BG104C =
SGlO'ii-i =
eGI04C =
K0100 -
S T R

0.
C.
0.
0.
C.
C.
0.
I P
4921
"1440
6361
0
3467
2274
5741
P
"LE
L8
is
L3
LB
LS
L3
E R -:J

KYCSCGEN/>-R ;i
HYCRCGEN/I-R y
HYCRCGEN/HR U
w
HYCRCGEN/hS ,,
MYCRCGEN/HR :,
HYCRCGEN/I-R „
HYCRCGEN/i-R ',,'

-------
              APPENDIX A-12-7
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-2-7 (96 - 111 hours)
                     319

-------
                                                                                                                        4/24/74
                                                                                                                                    PAGE
CO
N>
O

i :
1 !
i.
4


STATUS REPCRT CF
OPERATING FERICO:
riTF: «/24/74



OPERATING CCNCITICMS FCP INTEGRATED CPERATICN CF S02
TIKE CF RECCRD: 3:15 t R«: TC 18:15


- PRCCESS ELAPSEC TIKE CF PcRICD: START Sc.CC HRS / ENC
HRS



111 .CC HRS
RECCVERY PROCESS






1
i
. ' 1
',|

LENGTH. OF PERICC: 15.00 HRS .;
.•
1' PROCESS VARIABLES FCR OPERATING PERICC:
t
•'- -3




S 0 2 SCR
B E R






:: -:
r-
li!
w
I.
•--
'_
—
6:15
11:22
14: 2
19: 2


6:15
12: 2
19: 2

HRS
H3S
HRS
HRS


H?.S
HRS
HRS

9<;.CO HRS <£T)
1C4.30 r~£. !ET)
1C6.1C HRS i£T)
111.80 HRS tET)
AVERAGE'.

{* C .1 r% U O C ' T T $
* 3 • '_. V • - 5 i .. ! I
104. £•: :-ss ;ETI
1C7.C.C r-r.S 
Cv -4
E
3:15
18:15
HRS
HRS
96.00 HSS SET)
ill. CO H^S !ET!
A V 5 R i G £ :
H20 CC(>
:
V
2:15
10:15
.3:15
4: 15
6: 15
9:20
11:15
14:20
HAS
HR S
HRS
HRS
HRS
HRf,
has
"5. CO HRS !ET)
1C3.CO HRS (ET!
in.c; Has ;ET-
AVERAGE:
97. CO HRS !ET>
<5<=.f.-0 :-3S SET)
1C2.10 H'-S !ET!
lCi-13 HP,i (£1 )
AVERAGE:
CsIF^CE PRESSURE CT.CP
CR FICE PRESSURE DRCP
CS FICE PRESSCiRS O^CP
CR FICE PRESSURE DROP
OR FICE TECPERATURE
CR FICE TE;J-rj5RATliRE
C^ FICc TEXce?ATl.'Rr
CR FICE T£!-'PERATCRE
CS rSCE T5XPERATURE
JQO_
5DP-
ICP-
!TL-
tTL-
!TL-
!TL-
1C) /
1C ) /
1C) /
1C ) /
1C) /
"id" /
1 C ! ' /
13 ! /
1C! /
1C) /
OPIC :TI
CPlCiT)
CP101T)
ACP10
TL 10175
TL101T)
"" TL10IT)
TL:C:T>
TL10 (T)
ATL10
=
=
•ss
=
=
ss
=
	 	 2.200
2. 30G
2.300
2.267
319.000
315 .COO
3C3.COO
J94.COC
293. COO
304.200
INCHES H.20
INCHES H20
INCHES K20
INCHES H20
CEG F
DEC F
CEG F
CEG F
CEG F
CEG F
..
:,
£
^

-„
'-,.
' ,. --
y
i ;
-1

P. 	



. 	


4:15
12:15
20: 15

4: 15
20: 15

4:15
12:15

	 	
HRS
HRS
HRS

HRS
HRS

HRS
HRS

— •* •
97.00 HSS !ET)
ICE. CO H=tS !£T)
"-.»-, «/- (_"C fCTl
TOTAL:
RATE:

97. CO HRS (ET)
112. CO HRS -
JCVi-
,'CV,-
" CV.—
11 ) /
111" /
"ll'i"/
11) /

12) /
12) /
12) /
12) /
12) /
12! /
121 /
12) /
CD111T)
"COlllTl"
con :~ !
:-:C 1 1
RD11

CD12!T)
CD12!T)
WD12
RC12
CW121T)
CW 1 2 ( T )
CW 1 2 ( T !
KCV.12
-
=
—
•±


—
=
.=
=
s
^
c.c
•» c/i ^
i.tOO
3.CCC
o.ias

0.0
0.0
o.c
0.0
o.c
O.C33
O.C45
O.C7S
LS CUST
LS CUST
L£ 3UST
L2 CUST
LE CUST/HR

L3 CUST
LE CUST
LE CUST
L3 CUST/HR
LS CUST
LB CUSi
L2 CUST
L3 CUST

tl
-
.,
.-
^
*J
-•3
:-.
'-
:

-------

12:
20:


4:
12:
2C:

15 MRS
15 h'R S
15 HSS


15 HkS
is vas
1= H3.S

.R A
97. co HSS
1CS.CO
H3.:o
A V 6

97. CO
1CS.CO
113. CO
A V E
r«S
rSS
R A
h-as
i-RS
f-SS
S A
T E :
!£T)
(£T)
CET)
G E s
(ET)
i£T)
(ET!
G E :
hEIC-HT
S TCT
3 TCT
14 TCT
z TOT

3 TCT
S TOT
S TCT
X TCT
C
S
s
s
s
s
s
s
s
;Ase
c\
c.\
T.N
c\
CN
CN
CN
'CN WEEPAG6
CYCLONE DL'ST
CVCICNS CLST
CYCLCNS CLST
CYCLONE CLST

CCLLECTCR CLST
CCLLECTCR CLST
CCLLECTCR CLST
CCLLECTCR ELST
<£K-
! D-
i C—
{ C-
{ C-

t c-
! 0-
{ C-
i 0-
12) /
11) /
115 /
11! /
11! /
12) /
12! /
12) /
12) /
RCK
cim.
C 1 1 ! 1 ,
Clltl,
t.-.\
D12C1.
Clttl.
C12S1,
ADI
12 =
T) =
T) =
1 f- —

T) =
T) =
T) =
2 A =
4/24/74 PiGE 2 ";
0.005 LB EUST/hR !
7.300 J (WEIGHT) }
7.220
7.1iO
7.227

7.300
7.220
7.160
7.227
3 <»=IGhT>
% (:•> SIGHT) •:'
3 (BRIGHT) ;
•j!
S (V.EIGHT) !•'
S (kEIGST) ;.;
J (WEIGHT) ;•'
S IXEIGHU ;.'
:
'*
•T
CO

-------
                                                                                           PA:
6"   0 I A
               CARBON
                                PRECO.NDITICNER
\
i
°
•>

-.:
?»"
; ;
V*
*-.
:f
-.-
i J "-
KJ ^
tO '"
CT
tsf,
S*
•»
b-!
^
-S
P*

P*
a»'
-*a
! J
Ui



5:15 HRS  rv.sr C^SEC .
S CN INLET CAR3C.',
CK INLET CAR8CN
ON INLET CAR3CN
ON INLET CARSCN
CN INLET CAR3CN
ON INLET CARBCN

CYCLCNE CUST
CYCLCNE O'JST
CYCLCNE Ct-ST

S CN CYCLCriS GUST
S CN CYCLONE OLST
S CN CYCLONE CLS"







1











(CS-3C1)
(CS-301)
(CS-3C1 )
;"s-3:i;
(C5-3C1!
(CS-3C1!
(CS-3C1)
tCS-301)
JCS-3C1 )
(CS-3C1 )

{ C-3C1)
C D-301)
( 0-301)
( C-3C1)

( D-3C1)
« 0-301)
{ D-301)



















/ Z301tl,T) =
/ Z 30 1 ( 1 , T ) =
/ Z 3 i 1 ( 1 , 7 ) =
/ Z3ti ::.T) =
/ AiiDli =
/ Z301I2.T) =
/ Z3C1I2.T I =
/ Z3CH2.T) =
/ Z331!2fT) =
/ AZ301E =

/ CC-OKT! =
/ CCSCliT) =
/ KD331 =
/ RC3C1 =

/ C301(1,T) =
/ D301(ltT) =
/ AD301* =



















8.560 *
3.C60 S
s.540 ;
• 6.100 ?
6.200 %
6.300 ?
c.^GC ?
6.250 S

0.0 L3
C.O LB
C.O LE
C.O L8

0.0 S
0.0 ?
0.0 ?



















(WEIGHT)
(-EIGHT)
(SciGhTi
(WEIGHT)
(HEIGHT)
(WEIGHT)
(WEIGHT)

CUST
CUS7
CUST
CUST/i-R

(WEIGHT)
(WEIGHT)
(WEIGHT)



















_;
	 .. ^
t
•y

--
j
. 4
'•s
,J
• J
•i
,*w
•»
rs
•i
^4
•s,
ti
'J
^
S*
ga
; i
-'\
hs
s*
M
y

;t
"»
'-*>
••<
'.,'
d
i
*^
iL-

-------
OO
N>
LJ
t
f
1?
,t
I

t
J
5;
'• -'
T
r>
•:'

'-»
p:
12
1
-.
'-..
:[.
'-i
-,
^
• :
~^_
34
^
"
^
'^
•4
..,
'«
„
-^
^
•*"
»-
V,
..
S-
0:15 HRS
6: 15 HRS
17:38 HRS

22:50 HRS
4:26 HRS
19:26 HRS
0:15 HRS
6:15 HRS
17:33 HRS
22:50 HRS
4:26 HRS
19:26 HRS

0:15 HRS
6:15 HRS
17:38 HRS


22:50 HRS
4:26 HRS
19:26 HRS


0:15 HRS
6:15 HRS
17: 3H HRS


' 22:50 HRS
4:26 HRS
19:26 HRS

C:15 HRS
6:15 HR S
17: 33 HRS
3-.1-. HRS
18:15 HRS


5:15 HRS
9:15 HRS
13: IS HRS
17:15 HRS


5: li HRS
9:i-: HAS
93. CO HRS ;ET)
S9.CC H-.S !£T!
lie. 43 HRS CETi
AV~R*^''""

91.60 HRS ;£T)
97.20 HRS (ET!
112.20 r-SS 1ST)
A V c R A G E :
93. co I-RS (ET;
99.00 HSS !ET)
11C. 40 HRS (ET)
AVERAGE:
91.60 hSS i£T)
97.20 H5S i£T)
112. 2C HRS !ET)
AVERAGE:
93. CO HR3 !£T!
99. CO H:>S !ET)
11C. 40 HRS !ET)
AVERAGE :

91.60 Has !£T>
97.20 rr.S t£T)
112.2C H?S ;3TS
. A V £ R A G E :

93.00 HRS (ET)
99.00 HRS SET!
11C. 40 r?.S (ET)
i V i R A G t :

91.60 HRS (ET)
97.20 HSS (ET)
112.20 HSS (ET)
AVERAGE:
93.00 HSS i=T'.
99. CO H^S (ET)
1 1C. 40 HRS !ET)
AVERAGE:
96. CO HSS ;£T!
111.00 rRS <£T)
AVERAGE:

93. CO HSS :£T)
ics.co HRS SET;
1C6.CC H5S JET)
liC. 00 HPS !ET)
AVERAGE :

95.CC .-:>. S !'£T!
SULFUR GE
S02 CC\C CUTLET GAS
332 CCsC CUTLET GAS
SC-Z CC.NC CUTLET CiS
SC2 CC:-,C CUTLET GAS

H2S CC.NC INLET GAS
H2S CCNC SNLET GAS
H2S CCNC INLET GAS
H2S CC!,C INLET GAS
H2S CCNC CUTLET GAS
H2S CC\C CUTLET GAS
H2S CCNC CUTLET CAS
H2S CC?.C CUTLET GAS
H2 CCI-C K.LET GAS
H2 CC\C IM.ET GAS
H2 CCNC If.LET GAS
H2 CCNC U.LET C-AS
H2 CC.NC CUTLET GAS
H2 CCNC CUTLET CAS
!-2 CCNC CUTLET GAS
H2 CC.NC CUTLET CAS

*-2Q CCN'C INLET GAS
H23 CC.NC I.NLET C-AS
H20 CC^C INLET GAS
H20 CCKC INLET GAS

H2C CCNC CUTLET GAS
H20 CCNC C'JTLST GAS
H20 CCNC CUTLST .CAS
H2G CLNC CUiLET C-AS

N2 CC.NC INLET GAS
N2 CCNC INLET CAS
M2 CCNC INLcT GAS

\2 CCNC CUTLET GiS
N2 CC\C CUTLET GAS
N2 CCNC CUTLET GAS
N'2 CC.NC CUTLET GAS
N2 INLET VCL FLC\\ RAT =
N2 INLcT VCL FLOU RJ"=
N2 I.NLET VCL FLCV. RA" =

% TOT S C.N INLET CARi:C?
5 TOT S CN IMLrT CiR -Z"
Z TOT S CS INLET CA!J.:!C>
3 TCT S C?v I.NLET CAS '.Zt
% TOT S CN INLET CAK:!C,'>

%, TOT S C.N Ct'TLST C.i.''. 2:*
% TOT S CX C-T-LET CA .--'t-
N E R A T C R
(GS-2C6)
!GS-2C65
{CS-2C-61

(GS-2CC)
(GS-2CC)
JGS-2CO)
(GS-2CO)
1CS-2CS!
•GS-206)
JGS-2C6)
-:GS-206)
ic-s-2co;
iGS-2CC!
JGS-2CC!
(GS-2CO)
(SS-2C6 !
JGS-2C65
:GS-2C6)
(GS-2C6)

JCS-2CO)
JGS-2CC)
(5S-20C:
«GS-2CO)

IGS-206!
55S-2C4!
? Gi— ^06 !

CGS-2CC)
iGS-200)
(GS-2CO:
* G -— 2 - \j .
IGS-206)
JC-S-206)
IGS-2C6)
(GS-206)
( C-ZOO)
! G-2CO)
« G-200)

{CS-3C2 !
JCS-3C2!
{CS-3C2!
(CS-3C2 )
(CS-3C2)

1CS-2CC!
/ Y206U.T) =
/ Y206!ljT! =
/ Y2Cr:i,T) =

/ Y2CC!2,T) =
/ Y2CO!2,T) =
/ Y2CO!2,T) =
/ Y2C6i2>T) =
/ Y2C6 '.2, T ! =
/ Y206(2,T! =
/ AY20cH =
/ Y2CCC3.T ) =
/ Y2COi3,T) =
/ Y2CO(3,T! =
/ AY2CCC =
/ Y2Cfc!3.T; =
/ Y2C6<3,7! =
/ Y206J2.T) =
/ 4Y2C4C -

/ Y2CC(4,T) =
/ Y2CCI4.T) »
/ AY20CC =

/ Y206«4,T) =
/ Y2C6;-. , T ) =
1 M^J^-.'Ci» —

/ Y2COI5.T) =
/ Y200I5.T) =

A Y ^ C <. r —
/ Y2C6i5,T) =
/ Y2C£(5,T! =
/ Y206(5,T) =
/ AY206E -
/ G2CC-. 5,T) =
/ G2CCt5,T! =
/ AG200E =

/ 23C-2!I,T> =
/ Z:C 2(1,7) =
/ Z3C2::,T ; =
/ A2302A =

/ y:c!i;-; =
4/24/74 PAGE 4
1.530 % (VCLUMEI
1.4CC 3 (VCLU^E) :
1.467 ? (VCLUME! :
.
26.000 1 (VCLUMEI
26.800 S (VCLUME)
25. COO ? (VCLUKE)
25.933 ? t VCLUME)
0.0 ? (VCLUK6) -j
0.0 ? (VCLUME!
o.o s ivcLuys) -:
0.0 ; (VCLUKE) . -i
0.0 S (VCLUNE) W
0.0 S (VCLUKE)
0.0 ? (VCLUKE)
0.0 % IVCLUCE) -'
C.C ? (VCLUKE) *>
0.0 S (VCLUME)
0.0 S (VCLUHE) n
C.O ? (VCLUVE) =
'-,
19.600 * (VCLU.XE) ~.
20.000 ? (VCLUHE)
22.300 % (VCLUMEI r.
20.700 ? (VCLUME! :,
W
51.300 X ! VCLUME) ii
50.500 ? (VCLU!'E) .,
52.430 ? (VCLUME) • -
51.467 3 (VCLUME) ;:
:-t
53.900 S (VCLUME) -t
52.300 ? (VCLUKE) ;„
52.100 S (VCLUKS) :-'
?2.933 ? (VuuU.-^£)
46.7.00 % iVCLUVE) ^
47.700 ? (VCLU.VE)
4.5.700 ? (VCLUMEI :i
46.700 ? (VCLUWE!
121.000 CFH (7C CEG F! '„
121.000 CFH (7C CEG F)
121.000 CFH (7C CEG F)
..
8.560 ? (VvEIGHT)
e.1'0 ? ('.EIGHT) :,
8. 060 * CoEIGHT)
8.540 %  EIGHT) «
8.325 3 (ViEICHT) ..,
.,
20. SCO ?. (v, EIGHT! ...
20. ico -. C..H:G:-TI

-------
                                                                                                                                      PAGE
U>
V

••-
'S
«
J —
•:
• j
F*. ,,,,
L4:
t'
;i
13:15 HRS
17:15 HRS
5:15 HRS
9:15 HRS
13:15 HR«:
17:15 HRS

5: 15 HRS
9:15 HRS
13:15 HRS
17: 15 HRS
5:15 HRS
9: 15 HRS
13:15 HRS
17: 15 HRS

ICi
lie
A
93
IC2
1C6
lie
A
1C2
1C6
lie
A
SE
1C2
1C6
IIC
A
.CO HRS SET)
.00 HSS SET)
V E R A G £ :
.00 HRf, (ST)
.CO !-KS JET)
.00 !-RS (E"T1
.CO HRS 
!CS-302) >
(CS-2CO) /
CCS-2JG) 1
(CS-2CO) i
JCS-2CC) 1
JCS-2CG! i
iCS-2CC! i
(CS-2CC! ;
iCS-2CO> t
JCS-2CO) >
(CS-2CO! 1
' Z2CC(i,T) -
Z2CCI 1,T) =
AZ200A =
' Z3C2(2,T) =
' zsoaUiT) =
' Z302I2.T) =
' Z302I2.T) =
AZ3C2B »
r Z2CO\2,T) =
' Z2CC'.2,T) =
' Z2COI2.T ) =
' Z2CCI2.T) =
' AZ200E =
' 2200(3, T) =
' Z200 !3,T! =
' Z2CO!3,T) =
' Z2CO(3,T) =
' AZ2CCC =
20.
19.
19.
6.
6.
6.
6.
6.
2.
2.
2.
t .
2.
2.
2.
2.
2.
2.
000 S
3tO S
99C ?
100 %
200 S
330 J
400 3
250_|_
300 %
300 ?
tcb's "
too ;
450 ?"
700 3
300 S
210 3
740 ?"
437 S
UEIGHT)
(Vi EIGHT)
IV,EIGIJT)
IV.EIGHT)
(ViEIGHT)
(WcIGhT)
( VvElGhT)
(V.EIGHT)
(WEIGHT)
(V.EIGS-T)
(WEIGHT)
(HEIGHT)
(WEIGHT)
(V.EIGHT)
( WEIGHT)
(WEIGhT)
(WEIGHT!
(WEIGHT)
i
;:
./
,.•
i
i
?
!V
	 ,'j
*
-rf

1
*• ;«:


t.'










:t
h . S
r* " -i
ir*' . '-»'
!*> • •»'
?:
i*'











•








:I.
^
TS :i
'-
r".
,


•
















• i
2.
"1

-------
to
to
t
i
i
v
;«.
;J
V
i;|
r*
; >
-:
'?
'-»'
hi-'
-V

u

r*

r;
£^
si
r>
'.£
r":
H
s*
^
3*
i :
: 	
! '
: ,'
r*
•tn

'-*
K
•,.
,j
•^
-
19:15 HRS
1: 2 HRS
21:15 HRS

v 21:15 HRS
3: 2 HRS
8: 2 HS.S
23: 2 HRS

19:15 HRS
l: 2 HRS
21U5 HRS
21:15 HRS
3: 2 HRS
8: 2 HRS
— "5 . *1 L-J C

21:15 HRS
3: 2 HRS
3: 2 HRS
23: 2 HRS
-
2 1 : 1 S HR S
3: 2 HRS
8: 2 HRS
23= 2 HRS
3:15 HRS
18:15 HRS

4:15 HRS
20:15 HRS



4:15 HRS
20: 15 HRS


5:15 HRS
9: 1* HRS
13: 15 HRS
17:13 HRS


3:15 HRS
13:15 H.*S
H 2
38.00 HRS t=T)
93.30 HRS (ET)
114. CO HRS 
ICC. 30 HRS (ET)
115. SO HRS (ET)
ft V E R A G E :
96. CO HRS (ST)
111.00 HRS (ET)
AVERAGE:
97. CO HRS (ET)
113. CO HRS (ET)
TOTAL:
RATE:

97.00 HRS (ET)
113. CO HRS (ET)
7 C T i L : ___
RATE:

93. CO HRS (ET)
1C2.CJ K-S CET!
ICS.OO r-RS (tT)
11C. CO H«S iET)
AVERAGE :

95. CO rRS (ET)
Ill.CC HRS iET)
A V E 3 A G E :
S GENERATCR/S
H2 CONC INLET GAS
H2 CQNC INLET C-AS
H2 CONC INLET C-AS
H2 CONC INLET GAS

H2 CONC C'JTLET GAS
H2 CONC 'CUTLET 'GAS
H2 CO\C" CUTLET GAS
H2 CONC CUTLET GAS
H2 CCNC CUTLET GAS

N2 CO,\C INLET GAS
N2 CCNC INLET GAS
N2 CONC I.SL5T C-AS
N2 CCKC INLET GAS
N2 CQNC CUTLET GAS
N2 CQNC CUTLET GAS
N2 CONC CUTLET GAS
f.-y f f \ f *"" n r ' C T f* A C
N2 CG.YC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CC.NC CUTLET GAS
H2S CONC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCIVC CUTLET GAS

HZQ CCNC CUTLET GAS
H2C CCNC CUTLET C-AS
H20 CCNC CUTLET GAS
H20 CCNC C'JTLET GAS
H20 CCNC CUTLET GAS
N'2 INLET VCL FLOV, RATE
N2 INLET VCL FLCh RST£
N2 INLET VCL FLOW RATE
iiEICHT CYCLCNE DL'ST
WEIGHT CYCLCNE DCST
HEIGHT CYCLCNE CtST
WEIGHT CYCLCNE CLST
•
ViEIGH.T FILTER CUST
hSIGHT FILTER CLST
WEIGHT FILTER CUST
WEIGHT FILTER..DUST..

% TOT S ON CYCLONE 2 jTT
% TCT S CN CYCLCNE C^-iT
? TOT S CS CYCLC.'-.S D-ST
? TOT S CN CYCLCME D JST
% TCT S CN CYCLC.NE C-ST

S TOT S CN FILTER OLiT
S TOT S C.\ FILTER CIST
•X. TOT S CN FILTER DLS'i
f L F L> R S
(GS-ICC) /
JSS-1CCJ /
(GS-1CC! /
 /
tes-iosj /

(C-S-1CS! /
IGS-1CE) /
JGS-lCg) /
jcs-icai /
JGS-iOS) /
{ G-ICC: /
( G— I C 0 i /
I G-ICC) /
t D-IC1) /
! C-1C1) /
'. D-1C1) /

{ D-102) /
J C-102) /
! D-102) /
t D-102) /

J 3-101) /
{ C-1011 /
! 0-101) /
t C-iDl i /
: c-ici) /

: D-1C2) /
! C-1C2) /
T R ! P -P £ R
Y10013.T) -
Y1CC!3,T! =
Y10G13.T! =
iYlOOC =

Y108(3tT) =
Y108!3tT) =
Y108I3.T) =
Y1C3(3,T) =
AY1CEC =

YiC055,T) =
YlCOIStT) =
YiC01;,T) =
AY100E »
Y108CE.T) =
Y108!5,T) =
Y 108! 5,7) =
Y>rc-c •»• i —
AY10SE =
Y1C8J2.T) =
Y1C8(2,T) =
Y103I2.T) =
Y1C3;2,T) =
AY10SE =

Y103(4,T) =
Y10Si4,T) =
Y1C8I4.T) =
Y106!4ST) =
AYioac =
G100i5,T) «
Gl£C!5,T) =
AG100E =
CD10KT) =
C010KT) =
W0101 =
R0101 =

CC1C2IT) =
CD1C2(T) =
V.C1C2 =
RD102 «

0101(1, T) =
C1CU1.T) =
D1CU1.T) =
AD1C1A =

C102I1,T) =
CiC2(l,V) =
A0102A =
4/24/74 PAGE 6 >
51.200 1 (VCLUfE) j
50.600 S (VCLUME) •]
51.000 ? (VCLUME) .1!
50,933 S (VCLUft) !ij
.
0.0 * (VCLUtfE) •-.
0.0 S (VCLUME) •
0.0 ? (VCLUHE)
0.0 S (VCLUtfE)
C.O S (VCLU.-'.E)
-3
46.300 S (VCLUME! '••:
49.400 S (VCLUME) «
49.000 ? (VCLU.VE) -',
49.067 S (VCLUME) <
52.200 % 1VCLUHE) •»
53.300 Z (VCLUf'E)
52.200 * (VCLUV.E) -»
c ? 500 2 ( VC1 L'K' c ! • •
52.500 Z (VCLUMEi »
28.100 S (VCLU.«E) -.i
23.600 * (VCLUf-E) r.
29,900 S ( VCLUKE) . tV
27.700 ? (VCLUME) -j
23.575 ? (VCLUfE) r.
"
19.300 S (VCLUME) a
17.-800 S (VCLUS'.E! b.'
17.600 ? (VCLUHE) »'
19.700 ? (VCLU.1E) :,
16.600 S (VCLUKE) ;;
121.000 CFH (70 CEG Fi ^
V21.0CO CFH (7C CEG F! .-s
121. OCO CFH (7C CEG F) ^
0.0 LB CUST J,:
0.0 L8 CUST y
C.O L6 CUST „
C.O L3 CUST/HR
.;
0.0 L8 CUST
C.O LB CUST
0.0 LS CUST
0.0 L6 CUST/HR
..-
3.520 Z (V.EIGHT) ^
2. 4 SO? (WEIGHT)
3.940 U (WHTGHT) .
3.340 S C* EIGHT)
3.695 ; ! HEIGHT) ,.:
•;
0.0 J (WEIGHT) „
0.0 '4 (HEIGHT) ;,.
0.0 ? (HEIGHT)

-------
                                                                          PAGE   7
C A F, 3  C  N
                INVENTORY
                                       H C ? ? E R
W— 	 5:
9:
: 13:
17:
S:
'; 9:
13:
17:
»

3:
13:
T*
-»•
•
-i
4:
=-' 1A :
=
15
15
15
15
IS
15
15
15


15
15



15
15

HRS
HP.S
HRS
HRS _
HRS
HRS
KRS
HRS


HRS
H.vi



H?.S
H.RS

98. CO
1C2.Q?
1 C 6 . G r-
iic.c:-...
A V E
98. CO
1C2.CO
1C6.CO
11C. CO
A V c

96. CO
' 1UCO
A V E



97. CO
107.00
T C
R
HRS
HP.S
HSS
R A
HRS
t/} IS) l/l
fir (V. •>'
J. J- 'X.
R A

.HSS
r".S
R A



H.XS
rSS
T
A
(ET)
!ET!
(HT)
!ET)
3 E :
(ET)
(ET)
(£T)
(ET)
G E :

(ET) (
;ET) C
G E : <



iET)
SET)
A L : !
T E :
RESICUAL S CN CARECN
RSSID'JiL S CN CAR6CK
R;s:;x'iL s CN CARDC:>
!>3S!C!JJL S CA CiKilCi.
RES-ICJAL S CN' CAR3C\
RESIO'JA'L H2C ON CARS'IN
RES-CUAL h2C ON CiRS'IN
RESIDUAL H.2C CN CAS3:N
RESIuJiL H2C 0\ C/5R2-.N
RESIDUAL H2C CN CA?,;t:tv

:ARSGN RECYCLE RATE
liXECN RECYCLE RATE
:ARSCN RECYCLE RATE

SULFUR C (

,3tGHT SULF'JR COLLECT;
.SIGHT SULFUR COLLECTS.

-------
                                                                                                                                            PAGE
u>
                                      STATUS RSPGRT  OF  OPERATING  CCNCITICNS  fC-: INTEGRATED  OPERATION  Cf S02 RECCVE3Y PROCESS
                             OPERATING  PERICC:

                             	D AT .£_:	4 / 2 A/ 74
                                   _U.?';E_G.F_ReCiR.C:	3tl.5_ H3S   TC  16:15 .HRS
                                   PROCESS  ELAPSEC TIME OF PERIOD:
                                                     START  <3t!.CC  HftS / ENC   111.CO I-RS
                                                                                                                   L'ENGTH OF~~PER7CC:   15.00  HRS
                  CF INTEGRATED PRCC5SS  ?ERFCR.VA,NCE:

_U_SQ.2.'~R"EyOVAL..

  Z.   h2~S~ LT'lTrfAT'lCN"

  3.   ACID CCNV = RS!Cr.  ITO  SULFUR)                  PVCS  =     73.22 % {ACTUAL)

  A.   HTTTlIlZATI CN~rTb~H2S)                    ~pFcTs~y~   69".32~3~f~ ~" ~                         PR~S~ = '~jr.^'''7V *-1 ACTUALl     '"
  	-----                                    ~   26.77"? (ACTLAt)

_6.	F2_ LI.- LIZ AT j C.N.A.". .UN 11	PUK-.2 _. -	l.CC. Cp_S	.	

j.	RESibOAL.SULFUR  CN'CAR£"CNT       ~           x90ATI°~"c~.c393Ta"s/is~c_	

~~tT.   CA R BClT R E CYCLE ~R ATT TC Si                     RC9 0  "^   29.163 LB~CTCB)/HR

_5,	AC 10 .LCACJNG ..IN.L.e.T_CAKECN_Vl_y5LU	J!.3Ci_C_.f	CiZ.23p_ie_A.CJC./L_8_C	

jo..	w5isfuR₯""ccT,:tEN'T'~INLET CARBCN  6"  UNIT  -     x'iO"IB »  ZE-Icl*2.JLsIff2c/1.8 c	

TF.   AC~I 6" Tc A ci NG~TM.~ E T'cTs iCN~8TnJNTT           xaolc"^"   cTzli" 3d~L"s~AC"i c7t s~c

_12.__y_QISTURJ CCNTE.\T INLET CARBCS  S"  UNIT	X302B -   C.C8A2 LB H2C/LB C

_13.	TQf AL~6CI C "cCNVEa"TED"B''''~UKlf             '  PVC   =~   15.30 ^	

"T*T  S"ULFU'R""CC'!;r

 15.	JULFLR  CC\
                                                                                                                50.0  S  (GCAL)
                                                                                                                5?.0  S  IGCAL)
                                                                                                                SC.O *  (GCALJ
                                                                                                              _lpp-.CJI_J_CCAL}_OF_SCR_8Ep S02	
                                                                                                                25.C 1  (GCAU  Or STRIPPEC"SCLFLR
               REPAIRED LciK IN  SULFUR RECIRCULATICN
             	P'u?-?  CN  SULFUR CC^.Cc'sSSR AT iCC.C-  HRS.
               LEVEL  IN" StLFLR"'.FCT_.CC>-N~FRC!l'.KCf_I.KAL..CF_
             _"?" hZC TO A""H2C	
               "REBUILT "SULFUR
                                                                                  .L3.4 HRS.

-------
STATUS REPORT  CF  OPERATING CONDITION'S FCR  HT!:CRATEO OPERATION CF SC2 RECOVERY PROCESS
OPERATING PES.'OC:
CVTE: 4/2W7* TICS CF RECORD: 3:
.
PROCESS ELAPSED TIME CF PERIOD: START

SLLFLS NiT£RI«L 31LANCE (USING PROCESS P2S1:

S 0 2

I N
INLET GAS AS SC2
::;L=T c AS RESIDUAL S
TCTAL IN:

CUT
CUTLET GAS AS SC2
CUTLET CARBCN
CYCLCNE C'JST
COLLECTCP. DUST
CiR3CN '«EEPAG =
r? TCTAL OUT:
00
6" DIA CARBO

IN _ .. ..
INLET CARBON
TCTAL IN:
CUT
CUTLET CARBON
CYCLCNE COST
TCTAL OUT:
S U L F U

I N
INLET GAS AS H2S (CYL)
INLET GAS AS H2S tPRCC)
INLET CAK3C.N
TCTAL IN:

OUT
	 CUTLET GAS AS H2S
OUTLET GAS AS SC2
CUTLET CAR3CN
TCTAL CUT:
15 hRS -

96. C' !



S C i

t G- 1 ; !
S C- 11)



t G- 13 >
t C- It}'
t C- 11}
< C- 12}
(Cu- it i

(RV-3CC.)
R C: E


( G-2i.:. I
( G-2C:. 1


( G-2C'')
i G-2 :r. i
'C 13:15 HRS

•RS / ENC 111.



S B E R

/ 3G1C4 =
/ ECU f- -
1 SI 10 »


/ 8G13A =
/ BC124 =
/ SOU A =
/ B012A =
/ BC1.12A =
/ S01C =
1 E C 0 N1 C I T


/ EC12A *
1 SI3GO =
/ SC201A =
/ BC3014 *
/ S0300 =
N £ R i T 0 R


/ 6G201B =
/ EG203R =
/ EC2C1A =
/ SI200 =


/ 6G2038 =
/ BC2C2A =
/ SC200 =


CO





2
^


C
3
0
0
c
3
I


3
3
3
0
3



C
5
3
S


C
c
7
7


"hRS "~





.35?2
.5047


.0784
.2639
.0135
.0
.ccos
.3614
ONE


.2689
.2539
. 2689
.0
.2689



.0
.4557
.2639
.7286


.0
.3150
.6825
.9975








Le
LE
LE


LS
Le
L8
LB
L2
R


LB
f a
LS
LB
LB



L3
L3
LB
L3


LB
LS
LE
L2


LEIVGTH Or PERICD: 15-CO HRS





SL'LFUR/r.R
SULFUR/HR
SULFUR/HR


SULFUR/h.R
SULFUR/hR
SULFUR/HR
SULFUR/hR
SULFUR/hR
SULFUR/hR


.
SULFUR/HR
SULFUR/HR
SULFUP./HR
SULFUR/HR
SULFUR/hR



SULFUR/HR
SULFUR/hR
SULFUR/hR
SULFUR/hR


SULFUR/hR
SULFUR/HR
SULFUR/HS
SULFUR/HR
j
\ 1
: (
;' i
.


; 1,
-.,
".-
- •>
3.
^
*
,
T>
.,
-J $
--* :
r* |
-t I
J 1
n i
-» -
=• !
-' 1
-., *
i,

M <
•2
•C
-;'
-I
'4
_
~-
^
^' i

-------
                                                                                                                                       PAGE 10
(jO
S3
VO

K 2 S
I N
INLET CARBON
"- •

CUT
CUTLET
CUTLET
£ L T ' c 7
CYCLCNE
FILTER
T


I N
INLET G
IKLET G
CUT
CUTLET
CYCLCNe
COLLECT
CYCLC,\E
OUTLET
CUTLET
OUTLET
T C T A


CARSCN
GiS AS
CUST
CUST
C T A L
.„.: 0


AS 18"
G 6 N E R

LIN:


H2S
S


OUT:
V_£ R-A.J- L

UNIT AS SC2
AS a" UNIT AS CYL
TCTAL

GAS 18"

A T 0 R /

"' ( C-2C2I

IS
LE
-
IB
Le
! 3
LE
LB


LS
Lc
I C
W. b
is'
LB
LS
LE
L5
iu oj oj en L'l ru
LB .
SULF'JR/FR
SULFUR/hR


SULFUR/rR
S'JLFUR/rR
SULrUR/HR
SULFUS/HR
SULFUR/I-R
SULFUR/HR



SULFUR/HR
SULFUR/HR
SULFUR/HR

SULFUR/hR
SLLFU?./hR
SULFUR/hR
SULFUR/rR
SULFUR/HR
Si-LFUR/!-R
SULFUR/I-R
SULFUR/I-R
SULFUR /1-R
SULFUR/HR
SULFUR/HR
SULFUR/HR
.:i
!,;
I:1
. i
'i

"1

•j]
s
'-„
r.
i,1
n
rz
.;
'.i
rs
t,1
:,
j,1
-
^

-------
                                                                                                                     PAGE  11

   NYORCGEN ViTERIAL  BALANCE:
                                           SULFL'R    GENERATOR
            J  *
                     INLET G/,S AS  H2         	t  G-2C':0  / 3G203C"=   _ 0.0 ""   lie HY
                    _!NLET_GiS AS  h2S_'!  / BC2033  ^_I_0.0     12 KYCRCGEM/i-R '
                     i'.LET GAS AS  H2S:?*CC>        ('3-2C:.V/ 2-203 "=     C. 3'i'lf IS" V.YCRCG £',/HS"
                     :N'.HT GAS AS  1-20                f  C— 2C2:l  / EG2C3D  =     G.:-A51 IS HYCRCGEN/rR
                    _:.'i:.S_T_Ci.*3C';	(  C-2C;. ;_/__6C201 h__f	C.•!05*_L2 rYCRCGEN/KR_
                            T C T  A L	I  N :	(RV-2CC)  /  Ht2CO  =     0.9917 LE~HYCRCG'EN/rR
           CUT
                    CLTfHT Gi.S  AS  '^2                I  5-2 ;.!•;  / EG2:05C  =      0,C     L8'HYCRCGcN/HR
                    C^'lH-T GtS  AS  K2S               (  G-ICt'>  / a02C:.H  =      C.O     Lc HfCRCGEN/f-.R

                   IpL_7l€T" C~:iSC'.                    ('~C-'2ci:7"/"BC202V~=      ~C.'l24J"CS~HYi:SCSEN/hS~
                        " "T"C f  &~L    OUT:     ~(RV-2C"«:T /"  1-02CO  =      0.3145 '\E~HYCRCC
                            H 2  S    ' G S  K  E R A  T  0 R ,' J.  U  L I- i; R'    STRIP
	IN       _	                     	
	:'.l£T CIS AS_H2	'	(_G-li;i)_ /_BG103C_=	0.4521 12 HYCaCO£N/!-R
	 "	  " "lr;L£LlCA=5CN		  _____   T C-2 :;;"! ^/_SC202H  =	'(
                            T C  T  A L     IN:      (P.V-!."!:!  /  hllOC  =     3.6162

           C L1  T	     .   __	       .	   	    	  	   	 .
                   _0-.'TLiT_GAS_>S_H2___	f. .G-lI'fl._/_SGsC4C  =	0-0     L5
                   _OL-T!_rT GiS_iS_H2S	,	t_G—1-.'• 5_-/_sGi04H  *	O.J411 L5
                   "ctTLET C*S  AS _r20	i~G-l :•'•")"/ 6G10'iC~=      'C.2'22l''_£
                          T"L T  A  L    "b'JT:      (RV- ICCi  /  hQICC' =      0.5632 L3

-------
              APPENDIX A-12-8
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-2-7 (111 - 126 hours)
                     331

-------
                                                                                                                                        PAGE   1
                                     STAr'jS 3EPCRT  CF  OPERATING CCiNCITICNS FCR  INVEGSATEO CPERiTICM  CF  SC2 RECOVERY  PROCESS
                            OPERATING  PERIOC:
                                - CATE:   4/24/7*
                                 CAT E:
                         _II£E_C_F _RECCRCJ	18:_15_HRS_ TC   24:  0_HRS .

                         _TI.UE  CF RECCRC:    0:  0 HRS  TC	9:15  rRS
	PS CC EC S . E L i?SEC _T_L'H_CF__P:R_!_CD_:	_ST A Rj___1 _1_1_..0 C H RS  /  EN5_'126.CC HRS
                                                                                                                LENGTH CF  PERiCD:   15.00  HRS
u>
u>



22: 15
2:15
6:50
10: 2

22:15
2: 15
6:50
10:15

18: 15
9:15


13:15
2:15
10:15

2L:20
23:26
2:15
4U5
6:20
9: 3


20:15
4:15


20:15
4:15

20:15
4:15




HRS
HSS
HRS

HRS
HRS
HRS
HRS

HRS
HRS


HRS
HRS
rRS

HRS
HRS
HRS
HRS
HRS
HRS


H:RS
HRS '


HRS
HRS

HRS
HRS




11 5. CO HSS SET!
119.00 HS? ;ET>
123.60 HRS 1ST)
126.30 HRS (ET)
AVERAGE:
115. CO HRS (ET)
115. CO >-
-------
                       20:15 HRS   113. CO H<*S  «ET )
                        «i"15 HRS   121.00 HRS  !=T)
                      _12:i5_hRS	129.CO HSSJET)	
                                     & v E R A'G e  :
                      Z TCT S CN CVCLCKE  DCS
                      2 TCT S CN CYC'-CNE  CLS
                      ?_TCT s CN CYCLCNE  cus
                     ""» TQT""S CK" CYCLCNE  ccs
                        A: 15 KRS
 U3.Cp_HRS_JET)_
_121.CO HRS  lEU
                       _12:1S  HRS	12S.CO HftS  (ET)_
                                         £ R
                                     A V
                                             AGE:
    . __          ^
TOt_S_CN_"CCLLECTCR Cl.ST
TOT S CN_CCLLECTCR Cl.ST
TOT'S CN CCLLECTCR CLST

! 0-
l C-
! C-
< D-
r j c-
r { c-
r i D-
r 5 c-

ii)
ID
11 !
11)
12)
12)
121
12)

/
/
/
/
/
/
/
/

cut
cut
Cll t

1
1
4h
I

,T> =
,T! =
, T ) =

7.
7.
6.
V
160
ISO
940
AClli « 7.093
012!
C12J
012i
i-t
l,T) »
T
1
D
,T) =
.T) =
12* =
7.
7.
6.
7.
160
130
940
077
2*7
j
I
*
S
j
«i
*
£
?
74 PAGE 2
(HEIGHT)
(HEIGHT)
(V.cTGH.7)
(VictSHT)
{V.EIGHT)
t KEIGHT)
( VEI GHT)
(WEIGHT)
>
1
!

\
j


A
'.•
'-,
CO
L-J
       p.
       ia
       k.
       y_
       it
       I "~

-------
                                                                                                                             4/24/74
                                                                                                                                         PAGE   3
U>
U»
-P-

i
1 • .
21: i s H5<; m,C->
1:15 HRS 113. CO
5:15 HRS 12Z.OO
	 . 	 9:1.5 hRS 	 126, .CO
i V C
6"
HSS t£T)
HRS :=T)
HRS_.LEI1 	
RAGE:
CIA CARBON PR
5 TOT S CN ir>0.£7 CARaCf.
S TCT S CN i.\LET CAREa.
X TOT S CN INLET CASECf>
% TOT S CN INL-cT CAP.BCN
? TCT S CN INLET CARECI.
E C 0 N D I T
 /
•«cs-3ci: /
ICS-301! /
vlE_^ 	
CC30HT) =
CC331CM =
WS3C1 =
"0301 =

D3C1(1,T) =
C30K1.T) =
AD301A =
5.900
6.93C
7.900
9. 100
• 450
C.O
C.O
0.0
0.0

0.0
C.O
0.0
? (WEIGHT)
S (WEIGHT)
J UEIGH'T]
X 1 W 1 1 un i l
LB CUST
L3 CUST
LB CUST
L8 CUST/HR

! (HEIGHT)
% (WEIGHT)
SS (WEIGHT)
•»•
1
f '
-t
• J
-J
4
9
••
-\
~»
z r:
X







ra
.' :.

-------
U)
La
01

n
U*
i '
;.;

»»
'>•>
*s
p
f*
-;•>
'.»
t •


t.
f.
ts-
9< .- '
'M'
51
^
J^
V
r"
^ • -
\f
•^
H
•*
.;
.-.

•J I
i:
^
•i
;.
SI
ITtJB H*S
2:26 HRS
8: 3 HRS

4S26 HRS
19:26 HRS
6:32 HRS
17:38 HRS
2:26 HRS
8: 8 HRS
4:26 HRS
19:2e HRS
6:32 HRS

17:36 H?.S
2:26 HRS
8: 8 HRS


4:26 HRS
19:26 HP.S
t:32 HSS


17:38 HRS
2:26 HRS
8: £ HRS
'
4:26 HRS
19:26 HRS i_
6:32 HRS
17:38 HRS
2:26 HRS
8: 8 HRS
18: 1 5 HRS. _
9:15 HRS


21115 HRS
ins HRS
StlS HRS
9:15 HRS


21:15 HRS
IslS hRS
11C. 40
HRS
IETJ
119.20 HRS SET)
124.90 HRS (ET)
AVERAGE :

97.20
_112.20
123. 30
A V E
110.40
119.20
124.90
A V e"
97.20
112.20
_123.30
A v' ~
115.20
124.50
a v_s.

97.20
112.70
123. iO
A.V E.

HC. 40
119.20
124.90
A V S

97.20
_112.2C
123.30
A V E
UC.40
119.20
124.90
A V E
111. CO
126. CO
A V £

114. CO
US. CO
122.00
126. CO
A V S

114.00
lie. co

HRS
HRS
H«S
R A
HSS
HRS
HRS
R A
HRS
HRS
R A
hSS
R A

:-*5
Si

-KRS.
HSS
R A
' v> i/>  •<
• ft. x ef
: JL a.;*, it
HRS
HRS
HRS
R A
.KPS

IETI
(ET)
iETJ
5 £ :
(ETI


G E :

:ET>
• ET)
i ? T ',
-P...5. :

.5ET1_
•3 E :

;ETI
!ETJ
G^E :
-IET).

(ET1
S E :
JET.L-
. < £J.)
RAGE:

HSS
HSS
hRS
HRS
R A
HSS
HRS

(ET5
(ET)
JET!
(ET|
6.5..:

(ET)
(£T>
SULFUR 6E
, S02 CONC CUTLET GAS
$02 CCNC CUTLET GAS
S02 CCNC CUTLET GAS
SQ2 CCKC CUTLET GAS

H2S CCNC
H2S CCNC
H2S CCKC
H2S CCN'C
H2S CCNC
H2S CC.VC
H2S COX
H.2S CCKC
K2 CONC
H2 CCNC
H2 CCNC
>2 CCNC
r2 CCNC
S-2 CCNC
H2 CSNC
H2 COKC

H20 CCN'C
H2C CCNC
t-2C CC'.C
i-20 C.CNC
H2Q CCNC

INLET GAS
INLET GAS
INLET GAS
INLET GAS
CUTLET GAS
CUTLET GAS
CUTLET GAS
CUTLET GAS
IMET GAS
INLET GAS
INLET GAS
INLET GAS
CUTLET GiS
CUTLET GAS
CUTLET GAS
CUTLET GAS

INLET GiS
ISLET GAS
INLET GAS __ _.

CUTLET GAS
H20 CCNC CUTLET GAS
H20 CC.\C CUTLET GAS
H20 CCNC CUTLET GAS

N2 CCNC
M2 CCNC
_ M2 CCNC
\2 CCNC
N2 CCNC
K2 CCNC
•V2 CC?,C
N2 CCNC
N2 INLET
N2 INLET
K2 INLET
.
t TCT S
S TCT S
S TOT S
% TGT S
	 ?_TCT .S.
* TOT S
S TOT S

IMET GAS
INLET GAS
INLET GAS
INLET GAS
CUTLET GAS
CUTLET GiS
CUTLET GAS
CUTLET GAS
VCL FLCb RfT£
VCL FLO'« F:/'"E
VCL FLC1. f./Vg

CN INLET c#r -:CN
CN INLET c*= :;c;-.
CN INLET CAf.«CN
CN INLET C/il.::CK
CN INLET C.!P ::;N

CN CU7L = T C.-:=C\
CN CUTLET C i:=CN
N E R A T C
(GS-206J
R

[GS-2CO
IGS-20C)
{GS-2CO
fGS-2CC)
JCS-2C6)
(GS-206)
(GS-206)

:GS-2CC
{OS-?. CO
SGS-2CC)

JGS-2C6)
JC-S-204 5
SSS-2C6)

fGS-2CO!
CGS-2CC)
:GS-2CO)
CGS-2CC)
SGS-2C6!
 .-,
I (VCLUME) -,
,t
j ivcL'jys) .;
S IVCLUi-'i) --
? i VCLUME) -,
-e
? (VCLUME) .-,
? ( VCLUME i
% (VCLUM;) .,

? (VCLUVE)
? JVCLUXE:
? i VCLUME)
S (VCLUKEI ..
1 (VCLL'XE) e
1 (VCLUVE!
? 1 VCL •„••• = !
1. (VCLL.Vs! ,
CFH (7C CEG F)
CFH (7C CEG Fi
CFH !7C CEG F)

S (k EIGHT!
n < •« s : c •f T >
" I •« E I G H. T I
•' ( V. = J G !- 7 )
? ( ;•. E I G v 7 )

? ' s- S i G :- T )
? IkcICr.T)

-------
CO
Co
i.
3:
'.2' \
'•
*'
i
I'i
H

fv ,
*»
f
f

•s
y
;i
f-
r
j;
0-

3
iu
as
5*'
2»
U


b '



«
fl-t

1^
.r
5:15 HRS 122.00 '-RS (ET)
9: 15 HRS 126. CO r^S (£T)
AVERAGE:
2U15 HRS 114.00 HRS !£T)
1:15 HRS u s. eo HRS (FT)
5: 15 HRS 122. CO HRS (ET)
9:15 HRS 126. CO HRS 1ET)
AVERAGE:
21:15 HRS 114. CO HRS (ET)
1:15 HRS 113. CO HRS (ET)
5:15 HRS 122.00 HRS (ET)
9:15 HRS 126.00 HRS (ET)
AVERAGE:
21:15 HRS 114. CO HRS (ET)
1:15 HRS 118. CO HRS (ET)
5:15 HRS 122.00 HRS (ET)
9:15 HRS 126. CO HRS (ET)
AVERAGE:

























% TOT S CS CUTLET C*U!CN
S T:T s CN CUTLET CA^CN
S TOT S CN CUTLET CA»;!CN
? H2C CN INLET CAR8C\
% H2C 'CS INLET CAR3C\
% H20 CN INLET- C'AROC\
* H2C .CN INLET CAREC.N
Z H2C CN INLET CAR5C\
2 H20 CN CUTLET CARSIN
? H2d CN CUTLET CAREZf.
Z H20 CN CUTLET CAR2C!.
S H20 CS CUTLET CAREt;,
% H20 CN CUTLET CARS:i,
Z ACIC CN CUTLET CAREEN
2 ACIC CN CUTLET CAR3.:N
* ACIC CN CUTLET CARECN
2 ACIC CK CUTLET CAR3CK
S ACIO CN CUTLET CAR2CIV










,









.




ICS-2CC) / 2200(1. T) =
•CS-2CC) / Z2COI1.T) =
(CS-iCO) / AZ200A =
(CS-302) / 2i:2!2-T! =
(CS-3C2I / Z2C2(2TTi =
JCS-3C2) / Z3C2(2,T) =
(CS-3C2) / AZ3C28 =
CCS-2CC) / Z200(2,T) =
ICS-2CC) / Z20C'.2,T) =
(CS-2CO) / Z2CC(2.T) =
SCS-2CC) / Z200'.2fT! =
JCS-2CC) / AZ20CE =
(CS-2CO) / Z200(3,T) =
(CS-2CC) / Z200O.T) =
(CS-2CO) / Z20C(3,T) =
ICS-2CC) / Z2CC(3,T) =
ICS-2CO) / AZ200C =




















-
•
•


4/24/74 PAGE 5
19.640 5 (WEIGHT)
19.960 ? (WEIGHT)
19.640 % (WEIGHT)
5.900 ? (WEIGHT)
&.900 J (WEIGHT)
7.900 1 (WEIGHT)
9.100 ? (WEIGHT)
7.450 % (WEIGHT)
2.900 I (WEIGHT)
2.400 S (WEIGHT)
2.800 S (WEIGHT)
3.200 ? (WEIGHT)
2.825 S (WEIGHT)
3.040 S (WEIGHT)
2.400 * (WEIGHT)
2.350 * (WEIGHT)
2.450 ? (WEIGHT)
2.560 S (WEIGHT)

























I
i
J

it
'',<
'.'
!;!
-.1
';.'
T-I
•J
' t

w
•-.•
1
n
. i
„
-i
'-i
-'
-j
'•*
^
i
..
ts
:•«
-
^
j
'
-------
                                                                                                                          4/24/74
PAGE
                                                   H 2  S
                                                                 N E R A TOR  /
                                                                                    tJL F U R
                                                                                                 STRIPPER
U>
u>
l: 2 HRS
21:15 HPS
4:45 HRS

6:15 HftS
23: 2 HRS
3:50 HRS
9:26 HRS

1: 2 HRS
• 21: 15 HRS
4:45 HRS
6:15 HRS
23: 2 HRS
3:50 HRS
9:26 HSS
6:15 KRS
23: 2 HRS
3:50 HRS
9:26 HRS
6:15 HRS
23: 2 HRS
3:50 HRS
9:26 HRS
18:15 HRS
9:15 HRS

20:15 HRS
4:15 HRS



20:15 HRS .
4:15 HRS


21:15 HRS
1:15 HRS
5: 15 HRS
9:15 HRS


18:15 HRS

115 HRS
93.80 HSS 
121.00 HSS (=T)
TOTAL:
RATE:

114. CO HRS (ET)
113. CO HRS !ET!
122. CO HSS !ET)
176. CO H5S !£T)
AVERAGE:

11 '..CO HRS tET)
** *?#• 0 "} ^ ^ ^ ' ^ ~ )
A V ERASE:
(-2 CCNC INLET CAS
H2 CCNC IKLET GAS
H2 CCNC SKLET GAS
HZ CC\C INLET GAS

K2 CCNC CUTLET GAS
H2 CONC CUTLET GAS
H2 CONC CUTLET GAS
>2 CCMC CUTLET GAS
H2 CCNC CUTLET GAS

N2 CCKC INLET GAS
N2 CCKC INLET GAS
M2 CCKC INLST GAS
N2 CCNC INLET GAS
N2 CCNC CUTLET GAS
N2 CONC CUTLET GAS
S'2 CCNC CUTLET GAS
N2 CGN'C CUTLET GAS
M2 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H20 CCN'C CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H2Q CCN'C CUTLET GAS
i-20 CCNC CUTLET GAS
N2 IN-LET VCL FLOW RATE
N2 INLET VCL FLOS* RATE
N2 INLET VCL FLOW RATE
HEIGHT CYCLCNE DLST
hEIC-HT CYCLCNE CUST
HEIGHT CYCLCNE CUST
WEIGHT CYCLCNE OLST

WEIGHT FILTER CLST
WEIGHT FILTER CUST
fcrlGHT FILTER CUST 	 	
. W?!GHT FILTER OUST

% TOT S CN CYCLONE DUST
% TOT S CN CYCLCNE CLST
S 7DT S CN CYCLONE OUST
% TCT S CN CYCLCNE CtST
% TOT S CN CYCLCNE CLST

S TOT S CN FILTER OUST
* TCT S CN F'LTcR DL-S't
% TOT S CN FILTER CLST
(GS-1CO) / Y100(3,T) =
tGS-ICO) / Y1CC!3,T) =
1GS-1CO) / Y100(3,T) =
(GS-1CC) / AY1CCC =

«GS-108) / Y10B!3,T) «
IGS-iOS) / Y108t3,7> =
 / Y10S(4,T) =
JGS-106) / Y1C6(4,T> =
{GS-1C8J / Y1C6<4TT) =
JGS-103) / Y10S(4,T) =
5GS-108I / AYiCSO =•
( G-1CC) / G10CI5.1) =
t G-1CO! / G100(5,T) =
I G-100) / AG10CE =
< D-101 / C010KT! =
(0-101 / CD10KT) =
( C-1C1 / «0101 =
( C-101 / ftClOl =

« D-102 / C0102(T! =
( D-102 / CD1C2IT) =
( C-1C2 / v;ci02 =
? D-102 / RC102 =

( 0-1C1) / ClCl(lfT) -
! 0-101; / 0101(1, T) =
? D-lCi; / CiOiEltTi »
( D-1C1) / CICKi.T) =
1 D-1C1 ) / A0101A =

( 0-102) / CIO 2! 1,7) =
i 0-1C2 1 / C.102 i • ,7 ) =
{ 0-1C2) / AC102; =
50.600 t (VCLUKE)
51. COO J (VCLUME)
50.700 3 ! VCLUKE)
50.767 * (VCCUKE)

. 0.0 1 (VCLUME)
0.0 ? ( VCLUKE)
0.0 % (VCLU"=)
0.0 5 (VCLUME)
0.0 S ( VCLUME)

49.400 % ( VCLUME)
49.000 S (VCLUME)
49.300 J (VCLUME)
49.233 S (VCLUME)
52.200 ? (VCLU.XE!
52.200 S (VCL'JXE)
52.603 3 (VCLUME!
52. iOO % iVCLUMt!
52.425 S (VCLUME)
29.900 S t VCLUKE)
27.700 * (VCLUME!
26.300 3 (VCLUMJ)
26.500 Z (VCLUKE)
27.725 S (VCLUME)
17.600 ? (VCLUME)
19.700 % (VCLUME)
20.200 ? (VCLUME)
20.600 ? I VCLUME)
19.525 3 I VCLUKE)
1Z1.C03 CFK (7C CEG F)
121.000 CrH (7C CEG F)
121.000 CFH (7C DEC F)
0.0 LB CUST
O.COS LB CUST
O.C06 L6 CUST
O.C01 LB CUST/HR

0.0 LE CUST
0.0 LB CUST
C.O LB CUST
0.0 LS CUST/HR

2.440 3 (HEIGHT)
4.CCC 3 (HEIGHT)
'..640 ? ('.EirtHTl
3.960 ? !V. = 'GH7)
4.010 ? (SEIGHT)

0.0 S (UEIGHT)
0.0 5 l'*-IGrT)
0.0 J (WEIGHT)

"
^
;,
f
;-;
-»
-T
:.
.-j
-j
.-
"4
/»
'•3
TJ
"3
;j
•''
7a
-0
TO
--;
-'•-*
;*
r*
Ti
j»!

i
_
-'3
-i
**,
'4*
-t.1
3
]l1
a
,;

.

-------
                                                                                                                                   PAGE
                                                             CARBON
                                                                            INVENTORY
                                                                                                 HOPPER
U>
CO
71:
1:
5:
9:


21:
1:
5:
9:

15
H<*S
114. CO
15 hRS 118. :0
15 HRS 12J.CO
1.5 hRS 	 126, CO

15
15
15
15


HRS
HRS
HRS
.HRS

A V E
" 114. CO
US. CO
12Z.CC
126. CO
A V E
HSS
HSS
H3S
R A
HPS
H5S
HSS
"R A
(ET)
I=T>
(ET)
J ET 1 	
G E :

(ET)
(ET)
!ET)
1ST)
G E :
^ RESIDUAL S ON CARBCN
S RESIDUAL S CH CAR3CN
s RESIDUAL s CM CARECN
t RESIDUAL S CN CA38CN
t RESIDUAL S CM CARBCN

% RESIDUAL H2C
S RESIDUAL H2C
t RESIDUAL H2C
* RESIDUAL H2C
% RESIDUAL H20

CM CARECN
CN'CASSCN
ON CAR6CN
ON CARECN
ON CARECN
?CS- 9C) /

T (WEIGHT) [i
I (WEIGHT) \'
— - I,
! (WEIGHT) 1.
? C«EIGHT)
? (ViEIGHT) '•
* ('.EIGHT) j.
S (WEIGHT) t>
iij
18:
9:
15
1.5
HRS
HRS
111.00
126. CO
A V E
HRS
HRS
R i
IET)
G E :
CARECN RECYCLE
CAP8CN RECYCLE
CAR3GN RECYCLE
RATE
RATE
RATE
1 C- 90) /
J C- 901 /
1 C- 901 /
C901I.T) =
C90(1,T> =
31.000
31.000
31. COO
L8 KAT'L/HR M
LB. PiT'L/HR --i
LE ^AT'L/HR ft
T«






S U L
FUR C C N
DENSER


•;?
'-^
22:
2:
6:
15
15
15
10:15




HRS
HRS
HRS
HRS


115.00
119. CO
123. GO
127.00
T

HRS
HSS
HSS
"HRS
0 T
R A
(ET)
(£T)
IET)

A L :
T E :
WEIGHT SULFUR
WEIGHT SULFUR
WHTGH.T SULFU3
HEIGHT SULFUR
WEIGHT SULFUR
WEIGHT SULFUR
COLLECTEC
COLLECTEC
CCLLECTEC
CCLLECTEE
CCLLECTEC
CCLLECTEC
S-401) /
S-401) /
S-401) /
S-401) /
S-401) /
S-401) /
S40KT) =
S401IT) »
S40K7) =
S40HT) =
. HS401 =
RS401 =
0.0
7.000
6.750
7.200
21.050
1.754
LB SULFUR j..
LB SULFUR *,
L6 SULFUR j,
LB SULFUR ij
L8 SULFUR ;V
L3 SULFUR/HR ~4
"*
a
sJ

-------
CO
Co
vo
f 	
I
4 •
•*• \
v
STATUS REPORT CF OPERATING CONDITIONS FC!
f'| OPERATING PERIOD:
>>'. CAT*: 4/24/74 TIME CF RPCCR£: 18:1? :
«'.
is!"
V
6
ni
\>L
CATE: 4/25/74 TIHE-DF RECCRC: 0: C :



PROCESS ELAPSED TIKE CF PERICO:
v
4/24/74 PiCE 8 '
: INTEGRATED OPERATION CF SC2 RECCVERY PROCESS i
i
•RS TC.
rRS TC

START lli.CC WRS
24
• 0 HRS
-.
9:15 HRS


END" 126.00 VRS LENGTH CF PERICO: 15.00 hRS
.
,
SUCVARY GF INTEGRATED PROCESS PERFGRKAMIE:

1.

S02 RSPQVAL

FRS02 >

•55. 3C

2

(ACTUAL) SO.C I (C-CAL)

-
?» - . -r
K
W
ft
N
s
w
2.
3.

4.

5.
6.
h2S UTP IZATICN
AC 1.0 CCXVERSICN (TO SULFUR)

H2 UTILIZftTICN (TO HZS )

SU.FLR RECOVERY
h2 UTILIZATION 4" UNIT
FVCS -

PH.CHS -

FRS '«=
FUH2 "
?9.B5
72.73

67.36

' 79.01
27.93
ICC. 00
X
2

X

 ?S.C % (GCAL)

JACTUiL) 50. C t CGCSLJ
,
(ACTUAL) 1CC.C * IGCAL) OF SGRBEC SC2
(AC'UAL) 25.0 S C GCAL ) OF STRIPPED SULFUR

"• »
,
•
,
23
;.
bj rj
y
*--
tr
y
•Q
£
L
1 ! '
35
H '
c:-
i ;
y-.
U


P
LJ
k-
U
7.
8.
RESIDUAL SULFUR ON CARBON
CASSCS RECYCLE RATE (CE)
9. ACIO LOADING INLET CiREC.N 6" UNIT

10.
11.
12.

13.
14.
15.







MOISTURE CONTENT IMLET CAR2CN 6" UNIT
ACIC LCACI.NG INLET CARSCti 8" UNIT
KBISTURE CONTENT INLET CARBCN 8" UNIT

TOTAL ACIC CONVERTED 6" UNIT
SULFLR CCM/ESSICS -TO HZS)
SULFUR CONDENSES EFFICIENCY


KAJOR EVENTS DURING OPERATING PERIOD:
PILCT PL^NT PLJCEC ON STAKC3Y AT
129.6 !-RS. TC CORRECT CARBON FE'EC
AT STG 6 CF THE 4" UNIT.

X90A »
RC90 »
X301C *

X301B "
X302C -
X302B -~

PVC
PSCI-S '
ERV400-



PR03LEM


C.C42S
2S.C44
C.2159

C.1C13
C.2I59
C.1C.13

84.36
£4.45
179.64






LB
LB
L3

LS
LB
LS

t
%
%






S/LE C
C!CB)/KS
ACiC/LB C

1-20/LE C
ACIC/L3 C
1-20/L8 C










I*
^1
-,
;,
X
•?'•
2^

'-4

..
.
..
-'
_..
.-
..
'r
'»•*






,







.;
.•

-------
i
1
Tii

»v — 	 	

i*


»*
iJ
N
i*
f*. 	

U
p
L
^ •
S.
C;-
?»
!*
it
STATUS REPORT CF OPERATING CCNCITIONS FCft INTEGRATED OPERATION CF SC2
OPERATING PERIOD:
CAT": 4/24/7* TIME C?"*£CCSC:
CATS: W2S/7* TIKE CF RCCCRC:

PRCCESS ELAPSED TIME CF PERICD:
18:15 !JSS
0: 0 HRS

START 111. CC
TC 24: 0 HSS
TC 9:15 KRS







HRS / END 126. CC fcRS
'i/2'./7<. PAGE
RECOVERY PROCESS



9

,
•;
LENGTH CF PcRICC: 15.00 HRS .,
SCLFUR K4TESI«U BALANCE (USING PRCCESS -H2S) :



! N
INLET GAS 4S S02
INLET C AS RES10U«L S
T C T A L IN:

CUT
OUTLET GAS AS SC2
OUTLET .CARBCN
CYCLCNE CUST
COLLECTOR OUST
C*RECh SEEPAGE
TCTAL OUT:
6" D 1 A C A


S 0 2 S C
( 6-' 13)
< C-- 11)
IRV-- 10)

I 6- 13)
1 C- 12)
C C- il)
t D- 12 >
CCfc- 12)
1RV- 1C)
R B 0 N P


R B E R
/ SGlOi =
/ BC11A =
/ SI10 =

/ BGI3A =
/ 3C12A =
/ SOU A *
1 8012A '
1 ECW12A =
/ SOIC =
R E C 0 N D I T



2.3257
1.2431
3.572E

0.1095
3.29C3
0.0133
O.C
O.CC04
3.^135
I C N



LE
LB
LB

LE
L3
LS
LS
LB
L6
E R



S'JLFUR/hR
SULFUR/HR
SULFUR/:-R

SULFUR/HR
SL'LFUR/l-R
SULFtS/l-R
SULFUR/FR
SULFUR/HR
SULFUR/HR

T
= 3
•1

('<
(J
--
"I
V


t<
^
_'
L, ~ • _,'
* IN - =
P
to
^
PS
i
S*
a* •
t '
to
r'
	 •- • •" • ••'
'**
1 ;• '
5 -
j..
Lr
Ui
U
•-
INLET CARSON
TCTAL IN:
CUT
OUTLET CARBON
CYCLCKE GUST
TCTAL OUT:
S U L

I N
ISLET GAS AS H2S (CYL)
INLET GAS AS S2S (PRCC)
INLET CARSON
TCTAL IN:

CUT
CUTLET GAS AS H2S
OUTLET GAS AS SC2
CUTLET CARBON
TCTAL OUT:
( C- 12)
• 1RV-3CC)

< C-2C1)
< C-301)
IRV-3CC)
FUR G E


1 G--2C1)
( G-2C1)
! C-2C1)
UV-2CC)


( G-2C5)
( G-3C5)
( C-2C2I
(U--2CO
/ BC12A =
/ SI300 =

/ EC 201* =
/ 80301A =
/ S0300 =
N E R A T C R


/ BG201S =
/ 3C203R =
/ BC201A =
/ SI200 =


/ 3G2055 =
/ 8G205A =
/ 8C202A =
/ S02CO =
3.2903
3.2903

3.2903
0.0
3.2903



0.0
5.2043
3.29C3
8.5952


O.C070
C.2491
7.7806
LE
LS

LE
LB
LS



LB
L8
LE


r- r- r*
m to n>
LE
SULFUR/HR
SL'LFUR/HR

SULFUR/HR
SULFUR/KR
SULFUR/HR



SULFUR /HR
SULF'JR/HR
SULFUR/hR


SULFUR /HR
SCLFUR/HR
SULFUR/HR
SULFUR/HR
-S

23
y
>
!o
U
U1
:'l
/U
-s
*,
:-'
H

fi

-------
4/24/74
PAGE 10

fi
H •
-4
':'
'.1
• 7;
?'
H
i,,
p
e
K
W
H
H
ij
r"

B
U
w
is
!
O -
H
U ,
u
H 	
34.
i .
i .
L
P

P=


U
i!".
L
i
H2S GENERA!
IN-
INLET CARBCN . -
T C T A L IN:
•
CUT
OUTLET CARBON
CUTLET GAS AS H2S
OUTLET GAS AS S
CYCLCNE CUST
FILTER CUST
TCTAL OUTt
OVERALL

I N
INLET GAS 18" UNIT AS SC2
INLST GAS B" UNIT AS CYL H2S
TOTAL
CUT
OUTLET GAS 18" LSIT AS S02
CYCLCf^E CUST 18" UNIT
COLLECTOR DUST IS" UffIT
CARBCN WEEPAGE 18" UNIT
CYCLCNE DUST 6" L'.NIT
CUTLET GAS 8" LNIT AS_H2S.._.
OUTLET GAS 3" UNIT AS SC2
CUTLET GAS 4" UNIT AS H2S
CUTLET GAS 4" U.'ilT AS S
CYCLCNE CUST 4" LMT
FILTER CUST 4" U.NIT
TOTAL S












r o R / s u i
i C--2C2) /
MRV-1CC) /
«

C--1C3) /
G--1C4) /
G- 1C4) /
D- 1C1) /
C-1C2) /
(RV-1CC) /
S L '. F U R


( G- 1C) /
( G--2C1) /
S U . F U R

J G- 13) /
Q- 11) /
3- 12) /
CVr- 12) /
0--3C1) /
G-2C5) /
3-:2C5.) /
G--IC4) /
G-1C4! /
C-iCl) /
C-1C2) /
U L r- U R











-
.FUR
8C202* =
SHOO =


BC103« =
BC-104B =
BG104S =
B010LA =
S0102A =
S0100 =
B A L J


8G10A =
EG 20 IE =
I N :

BG13A =
BD11A =
ECK12A =
E03C1* =
BG2053 =
8G205* =
EG104E =
3G1C4S =
BD101* =
60102* =
OUT:












STRIPPER
7.5244 L8 SULFUR/H.R
7.5244 LB SULFUR/HR


1.2431 LS SULFUR/HR
5.2248 LB SULFUR/HR
1.7542 Lfi SULFUR/HR
C.QOOO LE SULFUR/HR
C.O LB SULFUR/HR
8.2022 LB SULFUR/HR
> K C E


2.3297 LB SULFUR/HR
C.O L8 SULFUR/HR
2.2297 13 SULFUS/HR

0.1C95 LH SULFUR/HR
0.0133 LB SULFUR/HR
0.0 LB SULFUR/HR
O.C004 LB SULFUR/HR
O.C LB SULFUR/HR
O.C070 LE SL'LFUR/HR
C.2491 LS SULFUR/H.R
C.O LS SULFUR/HR
i.7542 L2 SULFUS/HR
G.CCCC L3 SULFUR/KR
C.O LB SL'LFUR/HR
2.1335 LS SULFUR/HR











_
1
y
: i
(4;
i-i
.*;
i •
i (
:»i

•-?
".
4
S1
	 . 1
•«!

I,'
jj
^
~i
'ci
f!.
-,
^
rS
i

-;
-fc
'"*
Us
1

.;
*<.
+f
•J
•"*
.-.

-------
                                                                                                                                   PAGc  11
U>
i
j HYC3CGEN MATERIAL BALANCE:
i
!'•

Is1
:•
i'!
»»
•i
\*'
H
•a
r
r"1
»-
y
73
v<
t-i
y
w --
Cd
P'1

I N
IMLET
INiLET
I?iL£T
INLET


•: u T
OLTLcT
CUTLET
CUTLET
DLTLET
T

I N
s u

GAS AS H2
GAS AS H2S JCYL)
C-iS iS H2S (PRCC)
GiS AS H2C
CAP3CX
TOTAL IN


GAS AS H2
GAS AS K2S
GAS AS H20
CAR3C.N
C T A L CUT
H 2 S GENE

INLET GAS AS H2
INLET
CUT
OUTLET
OUTLET
OUTLET
T
CASSON
T C T A L IN
GAS AS H2
GAS AS H2S
GAS AS H20
C T A 1 OUT
L.f U R C E
. •
t G-2C3J
( G-2(31
( C— 2C3)
! C— 2C3)
:  m ru

LE
LS
LS
LS
P
"L8
LE
LE
LB
LS
IB
LE
j
•' \
\
KYCRCGEN/HR
HYCRCGEN/HR -:
HYCRCGEN/rR
HYCRCGEN/HR t.
.1

HYCRCGEN/HR .>
KYCRCGEN/H-R -<
HYCRCC-E.V/HR •..;
KYCRCGEH/HR »•?
'.»
E R W
i_'
HYCRCGEN/HR al
HYCRCGEN/HR i.;
HYCRCGEN/HR '-,'
HYCRCGEN/HR '-j
HYERCGEM/HR ~i
HYCRCGSX/I-R k.
HYCRCGEN/HR ;,J
^ • 3S
-3
5-i S-'
BS
3-
1 ,










,







ZS
^

-'
U -=

M

-------
              APPENDIX A-12-9
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-2-8 (144 - 148 hours)
                     343

-------
                                                                                                                              PAGE  1
-C;
                                STATUS REFCRT CF CPERATING CCNCITICNS l:C-:-t  INTEGRATED OPERATIC* CF SC2 RcCCVERY PROCESS
/; 	 ~
i i
ii.
I4;
'j;
OPERATING PERIOD:
CAT=: 4/?t/74



PRCCESS


ELAPSEC TIfE
TtHE OF XECCRC: 3U '. HRS TC 7U5


CF PERIOD: START 14-V.CC hRS / ENO
HRS







I4S.CO HRS LENGTH CF PERtCC: 4.00 HRS
*•
if
PROCESS VARIABLES
FCR OPERATING PERICC:
v>
*•«
s?
)-;
i •
S-'
T*
!;
j2
a
LV
r1.
rs
S-
H
a

JS

"
t '
i/-'
;(,"

u

Ui


	


4:33
10:26

4:38
10:45
3:15
7:15


9:15
3:15
5:15
6:15
7:20
•4:15
12: 15

4:15
12:15


4:15
12:15



4:15
12:15

4:15


HRS
HRS

HRS
H.RS
HRS
HRS


HRS
HRS
HRS
HRS
HRS
HRS
HN»

HRS
HRS


HRS
HRS



HRS
H.RS

HRS
12: 15 HAS


145.40
151.20
A V 6

145.40
151.50
A V E
144.00
148.00
A V E

15C.CO
A V =
144.00
146. CO
147.00
148.10
A V E
145. CO
153. CO
T
145.00
153. CO
T

145.00
153. CO
T


145.00
153- CO
A V E

145. CC
.1.5 3. CO




HSS (ST)
HRS (ET)
RAGS:

HRS
HRS
=! A
"HRS
R A

HRS
R A
HRS
"HRS
HRS
"HRS
R A
..HRS
HSS
C T
R A
.HRS
HRS
0 T.
R A
HSS
HRS
G.T.
R A

H?.S
R A
HRS
HSS

JET)
(ET)
G E :
!ET>
(ET)
G E :

(ET)
G E :
(ET)
(ET)
(ET1
IET)
G E :
fET)
(ET)
A L :
T E :
(ET)
(ET)
i L :
T E : ..
(ET)
(ET)
A L :
T E :

(ET!
(ET)
G £ :

i£T)
(ET)
S C 2 SCR

502 CC'-.'C INLET r-Llt GJS
S02 CCNC iXLET FLLE G.SS
S02 CCNC INLET FLLE C aS

S02 CCNC CUTLET FLLE C-AS
S02 CCNC CUTLET FILE GAS
SC2 CCNC CUTLET FLLE C-AS
H20 CC-.'C INLET FLUE GtS
H20 CCK'C INLET FLUE G&S
1^20 CCNC INLET FLLL cos

CRIFICE-PRESSURE CfCP
CRIFICE PRESSURE 01 CP
CRIFICE TENFFRATU*!1
CRIFICE TEMPERATURE
CRIFICE TEfPERATLRi:
ORIFICE TEfFERATURi;
ORIFICE TEKPERATU*-:
WEIGHT CYCLCNE CUS f
WEIGHT CYCLC'NE CLSf
WEIGHT CYCLCNE CUSf
WEIGHT CYCLCNE DLST
WEIGHT CCLLECTCR DJST
WEIGHT COLLECTOR C'JST
WEIGHT CCLLECTCR CJ.ST
WEIGI-T CCLLECTCS CUST
HEIGHT C4RBCN WEEP«1E
hEIC-HT C*ReCN '.-rtEFA.'E
WEIGHT CARSCN WEEFA,;E
HEIGHT CARBCN KEEFAiJE

3 TOT S C.N CYCLC.1'E i^L'ST
1 TCT Z CN CYCLC.VE :-LST
S TCT S CN CYCLC^.£ '.'LET

S TOT S CN CCLLEC'Q-.l CLST
% TCT S CN CCLLEC'C.5 CUST
>» m* r r-v /" m i zr~ r-,"t r- 1 CT
B E R

!GS-
£GS-
(GS-

 /
i: : /
li 1 /

12) /
12) /
•• '• •> \ I


Y1C11.T) =
Y10I1.TJ =
AY10A =

Yl&tl.T) =
Y16C1,T! =
AY16*
Y10I4.T1 =
AY10D =

CPIO(T) =
AOP10 =
TLIO(T) =
TL101T) =
T| 1 T f T 1 =

TL10(T) =
ATL10 =
CD1KT) =
CDH(T) =
•KD11 =
RD11 =
CD12IT) = ,
CC12!T) =
WC12 =
SO 12 =
CW 1 2 ( T ) =
CVJ 1 2 '. T ! = .
KCV-.12 =
RCK12 =

Cllli-T) =
D i i ; i , ~ : =

C1211.T) =
C12il,T) =
*•>'?£ =




2COO.OOO PPH (VCLUKE)
1975.000 PPf (VCLUC.E)
1987.500 PPV (VCLUKE)

95.000
92.500
93.750
10.000
10. COG
10.000

2.300
2.300
315.000
301.000
313.000
20B.OOO
209.250
0.0
2. COO
2. COO
0.250
0.0
C.O
0.0
0.0
0.0
C.630
• 0.630
C.079

7-640
7.700
7 . i 7 •',

7.640
7.700

PPP (VCLUKE)
Ppy (VCLLKE)
PP.V (VCLU.'-IE)
? (VCLUHS)
S (VCLUKE)
J (VCLUHE)

INCHES H20
INCHES H20
CcG F
CEG F
CEG F
CEG F
CEG F
LB CUST
L2 CUST
L2 CUST
L2 CUST/HR
LE CUST
LB CUST
LE CUST
LB CUST/HR
LG CUST
L3 CUST
LB CUST
LB CUST/HP,

1 thcIGHTJ
! !V.£IG'-T)

? (V.EICi-1)
'i (XEIGHT)
'! ( ., c r r ^ T 1
                                 4 V  =

-------
                                                                                                                       4/24/74
                                                                                                                                    PAGE  2
Ol
                                                        C I A
                                                                 CARSON
                                                                                PRECOKCITIONER
I,
|;j

;i!
.
1 :
il-
w

f '
S*
K
H
-[••
L"!

F*
Q
M
6:15 HRS 147.
10:15 hRS 151-
A V
V
6:15 HSS 147.
A V

4:15 KRS 145.
12:15 HRS 153.


3:15 H.RS 144.
7:15 hRS 143.
A V



•




00
CO
c
GO
E

00
CO
T 0
R

03
00
E








HRS
HRS
R A
1-RS
R A

HRS
HRS
T
A

KRS
HRS
R A








!EI.)
(ET)
G E :
IET)
G £ :

(ET)
(ETI
A L :
T E :

t£T)
(ET)
G E :








* TOT S ON INLET CAP.ECI.
* TOT s ci« INLET CARECI.
* TOT S CK I-fcLET CARIC!.
S H20 ON INLET CARBCf
S H2C CN INLET CARBC^

WEIGHT CYCLCNE OUST
WEIGHT CYCLCNE CUST
HEIGHT CYCLCNfE OUST
HEIGHT CYCLCNE OLST

% TOT S CK CYCLCNE Dl.Sr
? TOT S CN CYCLONE Dt S "
Z TCT S ON CYCLCNE DLS"

.






(CS-301) ,
(CS-3G1) ,
• tCS-301) ,
JCS-301) ,
ICS-301) ,

I D-301) ,
( D-3C1) ,
! D-301) ,
{ 0-301) ,

t D-301) ,
( 0-301) ,
1 C-301) i








1 ZSOKltT) =
1 Z3CH1.T) =
1 AZ301A =
f Z30K2.T) =
< AZ301E =

f CC301ST) =
1 C030KT) =
f 1.0301 =
f R0301 »

f C301U.T) »
> C30KI.T) =
f A0301A -








7.860
9.030
8.470
7.000
7.000

0.0
0.0
0.0
0.0

0.0
0.0
0.0








91
?
«
J

LB
ce
LB
LB

3
J
J








CoEIGHT)
(•HEIGHT)
(WEIGHT)
(WEIGHT)
UEIGhT)

CUST
CUST
CUST
CUST/HR

IhEIGhT)
(WEIGHT) '
(WEIGHT)








j

4
.:
*
r
'9
'»
'-"
«i
-3
t
'.
-.-
-,
X
a
n
-,
3
        f
         ft-

-------
                                                                                                                              4/2(/74
                                                                                                                                          PAGE   3
                                                                    SULFUR
                                                                                    GENERATCR
Co
•P-

IS;
i1-
-
'S. -
f- , _. ,
k
ir-
w
H

cr
-s

:—
ST
i.
fc
i ;
br-
-
^
Jr
£
M
S*
C

to
1 !
JO
£•-'
**. *
i^ '
^
H-l




-•s.
17:38 HRS
2:26 H=.S
8: 8 HRS

4:26 HRS
i q- jf. fe9 c
6:32 HRS
17:38 HRS
2:26 HRS
8: 8 HRS
4:2fi HRS
19:26 HRS
6:32 HRS

17:38 HRS
2: 26" HRS
8: 8 HRS


4:26 HRS
19:26 hRS
6:32 HRS


17:33 HRS
2:26 HRS
8: 8 HRS

4:26 HRS
19:26 HRS
6:32 H?.S
17:38 HRS
2:26 HRS
8: 8 HRS
3:15 HRS
7:15 HRS


6:15 HRS
10:15 HRS

6:15 HRS
1C:15 HRS

HC.40
119.20
124.90
A V E

97.20
115 ">f\
123.33
A V E
11C. 40
119.20
124.90
A V E
97.20
112.20
123.30
A V £
HC.40
119.20
124.90
« V E

97.20
112.20
12.3 .30.
A V E

HC.40
119.20
124.90
A V E

97.20
112.20
123.30
A V £
HC.40
119.20
124.90
A V E
144.00
148.00
A V E

HRS
(-as
HRS
R t
HRS
HRS
HRS
R i.
HRS
HRS
HRS
R A
"HRS"
HXS
R A
HRS
H»S
?. A
HRS
i-RS
HRS
R A

HRS
"HRS
HRS
R A

(ET)
(ETI
(ET)
G E :

(EM
f £ T %
^ET)
G c :
(ETI
(ET) •
(ET)
G E :
— » ^ • t
!£T>
G E :
(E'i
!ET)
S E :

(ET)
(ET)
G E :

(ET)
!ET)
G £ t

HRS (ET)
HRS
HRS"
R A
HRS
HRS
HRS.
R A
HRS
HSS
R i

147.00 HSS
151. CO HRS
A V E R i

147. CO
151. CO
A V E
HRS
R A
JET)
!£T)
3 c •
(ET)
* (UTS
K2 INLET VCL FLCK R,U£
N2 INLET VCL FLCV> R.H£

S TOT S CM INLET CJRCCV
3 TOT S C.N INLET Ci.'.fC\
3 TCT S CK INLET C5 iftv

? TCT s CN CUTLET CI? = :N
% TCT S CN CUTLET O*S:t>
S TCT S CN CUTLcT CifETN
IGS-2C6) /
(GS-2C6) /
 =
Y2C&',4,T) =
AY20£0 =

Y200(5,T) =
Y200i5,T) =
Y200(5,T) =
AY200E =
Y206(5,T) =
Y2C6(5,T> =
Y2C6!;,T) =
AY206E =
6200(5,1) =
G20015.T) =
AG200E =

Z3C2(1,T) =
Z302(i,TI =
AZ302A =

Z200(1,T) =
Z2QOU.T) =
AZ200A =
1.400
1.21C
0.830
1.147

26.800
21.400
24.400
0.0
0.025
0.072
0.032
0.0
O.C
0.0
0.0
0.0
c.o
0.0
0.0

20.000
22.300
24.100
22.133

52.600
51.600
53.200
52.467

52.800
52.100
54.200
53.033
45.700-
47.200
45.6CO
46.167
127.000
127.000
127. COO

7.360
9.0SO
8.470

20.200
21.600
20.900
* (VCLUME)
% (VCLUME! :-.
I 1VCLUME) ]:,
S (VCLU.VE) i:!
.,1
S ! VCLUME) !:
S CVCLUME) •
J (VCLUME) 'i
? (VCLL'KE) '-,
S (VCLUME) t>|
S IVCLUXE) >
S (VCLUME! ~>
* (VCLUME) H;
S (VCLUKE)
2 (VCLUME) -.i
5 (VCLUME) r,'
; (VCLUKE) v
\ ( VCLUKE) ;,'
* 1 VCLUKE) a
.^
% (VCLUKE) ~~
S t VCLUME) W
Z (VCLUKE) _•
? ( VCLUKE) -,
^,
S (VCLUXE) -^
? i VCLUME) „'
S (VCLUKE) y
? (VCLUKE) y
jj
% (VCLUKE) =j
S (VCLUHE) ^
Z (VCLUKE)
S (VCLUME) -.,'
. 1
j*.
* (VCLUHE) LJ
* (VCLUHE) LJ
? (VCLUKE) ,j
S (VCLUKE) „;
CFH !7C DEG F) Ls
CFH (70 CEG F) J
CFH (7C CES F) L-j
|^
S (ViEIGHT)
3 (ViEEGHT) '
1 (V.EIGHT) •-.[
•;
? (WEIGHT) -.j
S (V> EIGHT) -^
% UEIGHT! .-.

-------
                                                                                                                   4/2t/T,
                                                                                                                               PAGE
                 6515 HRS
                10:15 HRS
 147.00 FRS (ET)
 151.CO rRS SET)
_AJ.'^E_R A_J5
                 6:15 HRS    147.00  HSS IET)
               _1PA1JLJ5*S	iSi.CO  ^RS t£Ti
               	     	1A  V  6  R A G E :
  % t-20 CN INLET CARS^
  % h20 CN INLET CARBCN
   . H 2C ...C N__LNL ET_C A R 8 C ? _

  S >-20 ON CUTLET CARECN
_S_1-2C ON CUTLET CaaeCK_
 _« h20_CN_CUTLEJl CARECK_
1CS-302) / Z3C2!2,T) =
(CS-302) / Z302(2,T) =
CCS-302) / AI302S =
5CS-20Q) / Z20Si2fT) *
(CS-2CC) / Z200i2,T) =
JCS-2CO) / AZ2CCB =
7.COC ? (WEIGHT)
7.000 S (WEIGHT)
7.000 ? (WEIGHT) t
3.200 J (WEIGHT) V
3.300 ? (VEIGrT) .-.
3.250 S (WEIGHT)
'*!
•
*
6:15 HRS
10:15 HRS

147.00 HRS
151. CO HRS
A V S R «

JET)
?£T)
G E :

S ACID ON
S AC 10 CN
S AC 1C CN

CUTLET
CUTLET
CUTLET

CARE^.
c«ne^
CAFfCN

ICS-200)
JCS-2CC)
IC5-2CO)

/ Z200!3,T)
/ Z200J3.T)
/ AZ20CC

E
'

1.470
1.850
1.465

* (WEIGHT) ;
S (WEIGHT) ;
s
£-

-------
                                                                                                                            4/24/74
                                                                                                                                         PAGE
CO
1
r:
|i
."_
.1
• t'
1* 	

j 1
1*
H
•4


ca
2'
is
!=:
=<•
P
l: 2
21:15
4:45

6:15
23: 2
3: 50
9:26

l: 2
21:15
4:45
6:15
23: 2
3:50
9:26
6:15
23: 2
3:50
9:26
HRS
HRS
hRS

hRS
HRS
hRS
HRS

HRS
hRS
HRS
HRS
has
hSS
HRS
hRS
hRS
HRS
hRS
ni 6:15 HRS
;.
;p
=
aJ
;J
ii.'


!4
23: 2
3:50
9:26
3:15
7:15

4:15
12=15


hRS
HRS
HRS
HRS
KRS

HRS
HRS


93.30
114. CO
121.50

99. CO
115.30
12C.60
126.20
A V E

93. BO
114. CO
121.50
a v E
99. CO
115.60
12C.60
126.20
A V E
99. C3
ii:.8o
12C.60
126.20
A V E
99. CO
115.80
12C.6C
12c.2C
A V E
144. CO
148.00
A_. V..E.
145. CO
153. CO
T 3
R
H
hRS (ET)
hRS (ET)
h^S (ET)
RAGE:

hRS IET)
hRS (ET)
h'RS IET)
hRS (ET)
R t G E :

hRS (ET)
hRS (ET)
hRS (ft)
SAGE:
HRS -:ET)
hRS 
(GS-1CC)
IGS-1CC)

(GS-108)
(GS-1CE!
IGS-1C?)
IGS-10E)
(C-S-106!


'>
ff
',-
RIPPER
Y100(3,T! =
Y1CC:2:T! =
Y1C3(3»T) =
AY1COC =

YlC3(3tT) =
Y103!3tT) =
Y:C6'. 3,T) =
AY10EC =

Y10015.T) =
YlOOtS.T) =
AV1CCE =
Y108I5.T) =
Y1CS(5,7) =
Y108(5,T) =
Y10815.T) =
Y1CSI2.TI =
YICS J2.T1 = "
Y10S12.T) =
Y 1 <~, fi i ? , T ) -
AY 1C SB =
Yice1, -*T; -
Y1C8J4.T) =
Y10S<4»T! =
AY 10 JO =
G100(;-,T) =
GlCO(5iT) «
AG10CE =
C2101 (7! =
XOIOI =
RD1C1 =
5C.600
51. CCO
5C.7;"
50.767

0.0
0.0
c.o
c.o
c.o

69.400
49. CCO
49.2CC
49.233
52.200
52.300
52.600
52.600
52.425
39. SCO
27.700
26.600
26.500
27.725
17.600
19.700
20.200
2C.400
19.525
127.000
127.000
127.000
0.0
G • 0
0.0
0.0
? (VCLUKE)
s CVCLUX;)
S (VCLUKE)

S (VCLUME!
* < VCLUME)
% (VCLUHEi
S (VCLUVE)
S (VCLUME!

? IVCLUHE)
? (VCLUVEJ
? IVCLU.VE)
? (VCLU.'-'E)
t (VCLUHE)
S (VCLUME)
? (VCLU'IE!
? (VCLUME!
t tVCLUKE)
S iVCLU.^E!
? (VCLUXE)
Z (VCLUME)
S ! VCLUME)
? 1VCLUV.S!
? (VCLUKS)
% (VCLLH;)
S (VCLUME)
S (VCLUME)
CFH (7C DEG F!
CFH <7C DcG F)
CFH <7C CEG F)
IE CUST
LB CUST
L3 CUST
LB CUST/hR


.
.-
t
7
1



-J
~t


•I
7

;j


...

33
.:;
-^
-*
i-j
•l

_.

P;
i .

-s'
*"
.-
.1*

4:15
12:15


6:15
10:15
3:15
7:15

HRS
hRS


HRS
hRS
HRS
hRS...
145. CO
153.00
. T. 0
R

147. CO
151. CO
A V E
144. CO
14 3. CO
A V S
HRS ;ET;
hRS !ET)
T ?. ! "
ft T £ :

hRS !=T!
RAGE:
HRS (ET)
h :: S 1ST)
RASE:
WEIGHT FILTER CLST
V.5IGKT FILTER OLST
V-'SIGh-T FILTER CUST
>.= IGhT FILTER DUST

S TOT S CN CYCLCNE CLST
% TCT S CN CYCLCNE OLST
? TGT S CN CYCLCNc CLST
t TCT S CN FILTER DLST
% TCT S CN FILTER OLST
% TCT S CN FILTER DLST
( D-102!
: 0-102)
S C-102)
i 0-102!

I 0-lCl)
5 D-ICi!
i D-101!
( 0-1C2)
t D-102)
I 0-102)
'
-' -
',
/
1
CD102ITJ =
CC1C2IT) -
^C1C2 =

Cl~l ( 1 , T I =
ClOlil.T) =
C1C2 1 1 tT ! =
C102tl,T! =
AD102A =
0.0
c.o
c.o
0*0

3. 860
3.EOO
3.3 30
0.0
0.0
0.0
LS CUST
LE CUST
LS CUST
LB CUST/l-R

% (-EIGHT)
? ;KEIGHT>
; (XEIGhT)
S U EIGHT)
S Cn EIGHT)
? (HEIGHT)
— 1
^S
fa
*-
-1
J
-'

LA

-------
                                                                '•/26/7't
                                                                             PACE
C *  R  8 C N
                 1NVENTCRY
                                        H  C
                                                 £ R
V 6:15 HRS 1*7. r.O l-RS !=T1 J RESIDUAL S CN CARBC!> ICS- 90) / Z90<1.T) =
f. 10:15 HRS 151. CO HSS  / Z90(2tT) =
!•! ic:i5 HRS 151-co HRS IFT» 2 RFsinuAi n?n nn c. is.tr*. TCS- 9O / Z90C2.T) =
'•: 18:15 HRS 159. CO rRS (ET) % RESIDUAL H2C CN CARfC.V (CS- SCI / Z90(2,T) =
AVERAGE:? RESICUAL H2C C.M C4!k!C;- SCS- 90) / AZ9CE -
;i'
3:15 HRS 144.00 r^S (£7! C4R3CN RECYCLE RATE •: C- 9C ) / C90 1 1 , T 1 =
> 7:15 HRS 1*3.00 h'KS IET1 CiSBCN RECYCLE SAT= 1 . C- 90) / C90il,T) =

Zi
-"
_.,
.
-J ' 	 —

•
,
_^
I
.,
.,
.
•-•
3. 300 ! (KEIGHT)
3.860 2 UcICHT)
3.830 t IWcIGrT)
2.100 % (WEIGHT)
2.900 J (HEIGHT)
1.700 1 (SicIGHT)
2.233 S (HEIGHT)
31.000 LB MAT'L/HR
31.000 LB PAT'L/KR
31.000 LB yAT*L/HR


0.0 L6 SULFUR
6.500 LE S'JLFUS
6.50C LB SULFUR
1.625 LE SULFUR/HR


-




'
















;
.:
,4
;-'i
' t
i
:a


'•<
^a
.:T
-«
f
;j
-2
:•*'
'*•
^
-,'
ai
.~-.
..
15
j*
-
_C

j
~!

^.
_^
*
,

..
•-

-------
CO
Ul
o
I
(
>•• 	
1 *
*-

STATUS RC-PCRT CF OPERATING CCNCITICNS
OPERATING PERIOD:
CATE: .4/26/74 TIf'E OF RECCRC: 3:1

.... PRCCESS Ft APSFT TK«F T.F PrRICC*:

START
4/26/74 PAGE 7
FCR INTEGRATED OPERATION OF 502 RECOVERY PROCESS
<• rsS TC 7:15 KSS

1'4.CC HRS / END 148. CO »-RS LENGTH CF PERIOD: 4.00 HRS
* . ,
.1
i'"
SLMXiRY CF INTEGRATED PROCESS PERFORMANCE: ' =
1. SC2 RSfCVAL
PSS02
* 95.23 s (ACTUAL: 9c.o * (GCAD




.«'
••-
-
^
•a
2. V2S UT I LI I iT !C:j
3. ACID CC:.VE-3IC\ I TC S'JL.-UR)
4. H2 LTILIZATICN (TO H2S)

5. SULFUR RECOVERY
6. t-2 UTILI:;.T;C:; 4" US:T

7. RESIDUAL SULFUR ON CARBON
PUf-2S
?ucs
PHCHS

pas
PUH2

X90A
99.85 S {ACTUAL) 95. C 3 (GCAL)
77.23 % (' CTU.'-!.) 9-'^#Lb-/tei~'W

C.C956 L3 H2C/LB C :
-
C.2294 LB ACiC/LS C
C.0956 LB S-2C/LS C ;
-
9C.29 S

= 8C.C3 % -
116.97 % . •
__

,
'
.
fi:TER
KG CFH ACTUAL.

-------
     9!
U1
1
i;i
!.;
V
!«.
:,l
STATUS REPCST CF OPERATING CCiVCITIONS
CPESATIfvO PERIOD:
CATE: 4/2*774 TIKE CF RECCRC: 3:
_
PRCCESS SLiPSEC TIME CP PERIOD: START

SULFUR MATERIAL BALANCE (USING PRCCESS H2S):
4/26/7^ PAGE 6
FtR INTEGRATED OPERATICN CF S02 RECCVERY PROCESS
15 hlS

1 4.CC


TC 7:15 HRS

HRS / END 148.


:
.
CO hRS LENGTH CF PEfUCD: A. 00 hRS :
t
i
i
r- 	 : 	 	 : 	 -:
r
r~
K__
h' -

S 0 2

: N
INLET GAS AS £02
INLET C AS RESIDLAL S
TCTAL IN:

; c

! :- 13)
< r- ID
tRs- 1C)

R 3 E R

/ 3G10A =
/ ECU* =
/ sno =



2.3A02 LB SULFUR/hR
1.1873 13 SULFUR/hR
3.5275 LS SULFUR/hR

~!~ C U 7
s
•zt
y
B*1*"
_
-..•
w
1 1
u
y •
**!
k*
v.
S
CUTLET S.'.S AS SCE
C'-TLET Ci?3C\
CYC' C^5 DUST
CDLL5CTCS OUST
CARBCN KEEPAGE
TOTAL OUT:
6" 0 I i _C A__B S C

I N
INLET CAS8CN
TCTAL IKS
CUT
OUTLET CAR3CN
CYCLCNE DUST
TCTAL OUT:
S U L F C
; :- is;
( f- 12:
( f- 12)
(C'.- 121
(RV- 1C)
!> P


I C- 12)
(?V-3CC!
( C-2C1)
i r-sci)
(F.V-3CCI
R G E
1 BC12A =
/ ED12A =
.' 8CK'12* =
/ SD1C =
S E C G N ~ I T


/ 8C124 =
/ SI3CO =
/ SC20H =
/ BD3CI4 =
/ S03DO =
X E R A T C R
C.1IC4 IS SLLF'JS/HR
3.365C LS SULFUR/HR
C-v LE SLiLFUS/hR r
O.C091 LB SULFUR/hR r
3.5075 LB S'JLFUR/hR -
: c N E s -
_
-
3.3688 L3 SULFUR/hR -
3.3638 LS SULFUR/HR ' ;
3.3683 LS SULFUS/1-S
0.0 LB SULFUR/HR
3.3688 LE SULFUR/HR ..
-
U
L-L
:.j
P '

^:
. _ — .. — . 	
r--
I N
INLET GAS AS h2S (CYL)
INLET GAS AS H2S tPROC)
INLET CARSON
TOTAL IN':

CUT
OUTLET GAS AS h2S
CUTLET GAS AS S02
CUTLET CAS8CN
TCTAL CUT:

{ 0-2C1)
1 1.-2C1)
( C-2C1)
t-!"-ZCC)


{ G-2C5)
( G-2C5)
t C-2C2)
1 t'--2CC)

/ BC2013 =
/ BG2C3R =
/ 3C201* =
/ SI2CO =


/ 3C205E =
/ S02CO =

0.0 LE SULFUR/hR
5.5679 LE SULFUR/t-a
3.3638 LE SULFU^/HR
3. 9367 16 SULFUr/hR

_
C.C07A LE SULFUR/i-R
3.2615 LB SULFCR/hn
8.1A44 L2 SULFL.R/HR
6.4133 L3 SULFUR/i-R
I?
a .... — ...... . ... .

-------
Oi
f 	 	 	 	
i
T:
*
.i'
••
'i
,t
f'
S
'7
w


-li
/ J

a
w
H
F*
s*
e»'
3>
'«
'. ' f
b*
-^,
fc
1^
r':
, 	 -.
lo
L-
1 1 	 . 	
1 r 	 	 — • 	
r'
. 	
H2S GEKERA
I N
INLET CAR^C?C
TOTAL IN: '

CUT
CUTLET CARBON
CUTLET GAS AS H2S
CUTLET C-AS AS S
CYCLCNE CUST
?ILT£R CUST
TCTAL CUT:
OVERALL

t N
INLET GAS IS" UNIT AS SC2
INLET GAS 8" UNIT AS CVL H2S
TOTAL
CUT
CUTLET GAS 18" UNIT AS SC2
CYCLCI\E CUST 18" L'NIT
COLLECTOR CUST 16" UMT
CARSCN V.EEPAGE IS" UNIT
CYCLCNE C'JST 6" LMT
CUTLET GiS 8" UMT AS H2S
OUTLET GAS 8« UNIT AS sc2
CUTLET GAS A" UNIT AS H2S
CUTLET GAS 4" UNIT AS S
CYCLCNt CUST 4" UNIT
FKTER CUST 4" LMT
TCTAL S










TOR/ S U L
t C-2C2) /
(RV -ICC) . /


1 C-1C3) /
( G-1C4) /
r G-lCn) /
( C-iCI) /
( C-IC2) /
(R'i--lCC) /
S L .FUR


( C— 1C) /
( C— 2C1) /
S '- . ? U R

( C— 131 /
i t- 11 > /
{ r- 12} /
(CV- 12) /
( [ -3C1! /
t C-2C5) /
i C- C5) /
( G- C4) /
( (.- C4) /
< L'-- Cl) /
'. t:-!C2) /
U L r U ft
,









F L R
SC2026
SI1CC


SC103A
3G104B
EG10R


SUS.FUR/i-3
SULFUR/t-R
S^,L^l.'i^/^?.
SULFUR/1-R
SULFUR/l-R



SULFUR/HR
SULFUR/I-R
SULFUR/l-S

SULFUR/hR
SULFUR/hR
SULFUR/rR
SULFUR/HR
S'.LFL'R/l-a
SULFUR/i-R
SULFUR/i-R .
SCLFUR/rR
SULFUR/hR
SULFUR/HR . •
SULFUR/t-R










\
•
'.

.
-



. -
"1
•j,
••
'-,
«
72
-t
:4
-'

r.
3,
Zl
^
,
;,
-
•-T
f-
a
-E
-»
.-
-t

-------
u>
t
1 HYD*CG£N MATERIAL BALANCE:
> S U L F
»3_ _
'•; IN
• = ' iNLET GAS AS H2
INLET GAS AS 1-2S (CYL)
'"' INLET GAS AS H2S (PRCC) -
I'' INLET GAS AS H2C
':•: IN' £T CARSON
-.-. • T C T A L I N :
:;i
;r CUT
?* OUTLET GAS AS H2
\i. OUTLET GAS AS H2S
p OUTLET GAS AS >-2C
'•. OUTLET CAR3CN
TCTALOUT:
\\
t'-.
'••- H2S GENERA
U IN
p INLET GAS AS H2
'si INLET CARBON
U.
~ - CUT
-.-. CUTLET GAS AS H2
i. CUTLET GAS AS H2S
to1 CUTLET GAS AS 1-20
e-- TCTALOUT:
r I
S-.
;s
'fc:
U



f=

L; R G E

t (,-:>C3)
( c-;:c3)
( c;-;!C3)
( G-,!C3>
( >;jci)
{RV-:!CC>


I C-;!C5)
< G-.2C5)
( :-.?c2)


T 0 =. / S U

< G-IC3)
( C-JC2)
CRV-1CC)
< C-1C4)
J G-1C4)
1 C-1C4)
iP'-lCC)









N E R A T C R

/ BG203C =
/ 8G203B =
/ BG203 =
/ 8G203D =
/ BC201H =
/ *I200 =


/ SG205C -
/ EG205H =
/ EG205C =
/ BC202H =
/ H3200 =

L F t R S

/ BG103C =
/ BC202H »
/ HIiOO =
/ BG104C «
/ BG104H =
/ SG1040 =
/ i-OICO =








4/26/74 PAGE 10


0.0 LE HYCRCGEN/1-R
O.C LE HYCRCGEf
-------
             APPENDIX A-12-10
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-2-8 (148 - 156 hours)
                   354

-------
OJ
Ui
     Ci
                                                                                                                      4/26/74


                                    STATUS REPORT Cr OPERATING CONDITIONS F:!R  INTEGRATED  OPERATION  CF  SC2 RECOVERY  PROCESS
                                                                                                                                  PAGE
I
!«:
OPERATING PERIOD:
CiTE: 4/26/74


TTJ'5 OF RSCCRC: 7:15 HRS

TO 15:15 HRS



':
.
•••: PROCESS ELi?S=C TtVE OF PERIM: START K.S.CC HRS / END 156. CO HRS LENGTH CF PERIOD: 8.00 HRS ;.
ft .
jti

PROCESS




',
VARIABLES PCS OPERATING PERICC: . !•
fi . >
i'= SC2SC-RBER
'**; ••
P
W

••»
L,'
10:26 «tS
14:26 HRS
13:15 HRS


10:45 hRS
14:32 HRS
IS: 15 H.RS
151.20 HRS (ET)
155.20 HRS (ET)
159. CO HRS (ET)
AVERAGE:

151.50 HRS (£T)
155.30 HRS (ET!
159. CO HRS !ET)
AVERAGE:
S02 CC.NC INLET FLUE 'iS
S02 CCNC INLET FLUE i..*S
S02 CCNC I.NLET FLUE 3*3
S02 CCNC INLET FLU'E 5*S

S02 CONC CUTLET FLUE GJS
SC2 CCNC CUTLET FLUE GiS
502 CC.NC CUTLET FLUE GJS
S02 CCNC CUTLET FLUE CAS
(GS- 1C) /
tGS- 1C) /
(GS- 10) /
tGS- 1C) /

!GS- 16) /

TOTAL:
SATE:
(-20 CONC INLET FLUE 0-KS (sTJ
161. CO K-S ;£Ti
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR OUST
WEIGHT CCLLECTCR CUST

WEIGHT CiRSCN WEEPiCE
WSIGH.T C/..-.ECN V.SEPiCE
V.EICKT CiRSCN '.vEEPtCE
WEIGHT CARECN W'ErP;C =

* TCT S CN CYCLONE CUiiT
S TCT S C.N CYCLCNS CUI-T
I TCT S C.S CYCLCKE CU5.T
( 0- 12) /
1 D- 12) /
5 D- 12! /
< C- 12) /

!CW- 12) /
:cv.- 12: /
«.Cl.- 12) /

-------
        f»



        (r

        I ;—
        h«
                                                                                                                            

-------
Ul
                                    _I51.CO. .KS

                                      4 V S S
 6"  OIA     CARBON

	?_JCT__S_.CN_ INL.ET

:    S TCT S  CN I'.'LET
                       _1C:15 Has	151.CO HRS  1ST)
                       _.1«:15 HRS	155.CO I-^S  (6T>
                       _1S_:15 HRS	153.00
                        2C:15
                         7:15  HRS
                        15:15  hR5_
  A V E S A G  6  :

__153.-0 !-.s!S..!cTi__
 161.00 J-RSjl£TJ	
"	T_C T_Ali_:	
       R"A T  £ ;

 148.CO rSS  (ET!

  A~~ v" 'E~T'~A~G' e'T"
     i H2o"oN"i\LEt"CARBON"
     S H20 CN  INLET CARBCN
     V h20~CV INLET ""
    _V.ZIGHT  CYCLC.'JE DUST	
    J»EJGHT_CYCLCKE CUST_J__
    _hEIGKT  CYCLCN'E'DUST   ' '
     ME IGh77~C'Y'Cl"CN£ DUST    "

     s  TOT s C.N CYCLCKE CLSV
    _S_T07_S C^_C^CLCNS_OLS"
     X  TO'r S~CN CVCLCNE DUST"
4/26/7* PAGc 3
PRSCONCITICNER
iCS-iCl) / Z3GU1,7) = 9.080 3 (WEIGHT)
iCS-30;! / Z3CI;l,TS = 9.niO ? ttiEIGH.T)
(CS-3C1) / AliOIi » 9.470 ? (kEIG^T)
(CS-3C1) / Z3CH2.T! = 7.000 S («£IGt-T)
ICS-3C1) / i3CH2,T) = 7.000 Z (UEIGHi)
{CS-3~1) / £331(2. T) = 5.603 S (V.EIGHT)
(CS-3C1) / AJ301E = 6.533 5 !V.£;GI-T)
{ D-3CI5 / CD301iT: = 0.0 L3 CUST
S D-301) / CD3:i:T! » 0.0 LS CUST
I D-30U / K3301 = 0-0 LS CL'ST
( C-3C1J / RD3C1 = C.O LS CbST/hR
r C-3C'n / DSOltltT) = C.O S thEJGhT!
S 3-3CI) / CSQUl.t) = C.O % {hilGhTJ
1 C-301) / AD30Li = 0.0 S IhEIC-HT)













,








1
T
.
!
=
I
C
• i

•r
-5.
: fc
- T
a
^
12
S3
-^
•J
-S
^
»
--'
-^
3S

r*;
io
!
-J
-.3
A*
-S
*^
-7
41
        fj

-------
                                                          4/26/7*
SULFUR
                  EMERATCR
^ 	
:'f
,1
V
*
i^
i 	 	
r:-
M
i-i
*<
::
;=
Li3 '**
Ln **
co H
'^-.
y
?.-
r
p-

•:!
c*!
•a

^,
;-'
^
U-
u
H


13:32 HRS
.. 14:56 HRS
	
13:32 HRS
., 14:56 HRS
13:32 HRS
14:5fc HRS


13:32 HRS
14:56 HRS


13:32 HRS
7:15 HRS
15:15 HRS


1C: 15 H~S
14: 15 HRS

10:15 HRS
14:15 HRS
13:15 HSS
10:15 HRS
14: 15 HRS
18:15 HRS
10:15 HRS
14:15 HRS
18:15 HRS

10: 15 HRS
14:15 HRS
IS: 15 HRS

154.30
A v E
155.70
V e
" 154.30
A V E
15.5*70
A V E
154.30
A V E
155.70
A V 6

154.30
A V t
155.70.
A V =

154.30
A V E
IAS. 00
156. CO
A V E

155.00
i V E

151. CO
155. GO
159. jO

151. CO
155.00
15?. CO
A V £
151-00
155. CO
159. CO
A V £
151. DO
155. CO
159.00
A V E
HRS 1ST)
RAGE:
HRS !ET)
AGE:
HRS 
HSS ;ET; . .
rRS (ET)
RAGE:
S02 CCNC CUTLET GAS
S02 CCNC CUTLET GiS
H2S CCNC INLET GAS
H2S CCi>C INLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET C-iS
H2 CGNC INLET GAS
H2 CCNC INLET GAS
H2 CGNC CUTLET GAS
H2 CCN'C CUTLET GAS
H20 CC.NC INLET GAS
H20 CONC INLET GAS

H20 CONC CUTLET GAS
H20 CCriC CUTLET GiS
N2 CCNC INLET GAS
N2 CCNC INLET GAS

N2 CONC CUTLET GAS
N2 CCNC OUTLET GAS
M2 IN'.ET VCL FLO* RA" =
N2 INLET VCL FLC'rf RATE
N2 INLET VCL FLGH RJ"E

Z TGT S CN INLET OSKSCN
s: TOT s CN I::LET C^P-::CN
X TOT S CN INLET CiRHCN

? TOT S CN- CUTLET C^=, tC\
% TOT S CN CUTLET CJI'.cCv
S TCr S Ci\ CUTLET C^-.£C<
% TCT S C.\ CUTLET C^KEC>
% H20 CN INLET CARBCIi
% H2C ON INLET CARSC:.
S H20 CN INLET CARSC.\
% H20 CN INLET C.1RBC.-;
S H2u CN CUT'.cT CAR2CI
? H20 CN CUTLET C*R3::r
S J-20 ON CUTLET CARB^
? H2C ON CUTLET CAR3'^
S ACID ON' CUTLET CA3:LN
? AC!D CN CUTLET C*' :CN
* ACIC CN CUTLET CA?3llN
% ACIC ON CUTLET CARKN
(G?-2C6)
iGS-2Ci!
!GS-20C)
(GS-2CO)
SGS-2C6)
1C-S-206)
{6S-2C01
JGS-2CC)
(GS-2C6)
(GS-2CO)
(GS-2CC)

tGS-206 )

(VCLUHE)
(VCLU«E)

(VCLUHE)
(VCLUME)
FK !7C CEG F)

:
	 '.

1
4
-}





n
'.t

CFH !7C CEG r)
CFH (7C CEG F) -•

i
9
^
e*
4
3
i
%
s
?

I '« EIGHT)
! WEIGHT)

(V.EIGHT)
!WcIGHT)
(HEIGHT)
("EIGHT!
(WEIGHT)
IViEIGHT)
(-EIGHT)
(weiGHT;
(hEIGHT)
(HEIGHT)
(HEIGHT)
(HEIGHT)
(l-EIGHT)
(V.EIGHT)
(V.EIGHT)
..

Z*
-

a
'*s


«»
^
^.
-*
"-
iS
a

-------
Ol
VO

*
1

«

>
*
7
i
i
-:
*
7:15
8: 8
12: 8
14:32

7:15

3: 3
12: 8
14:32
8: E
12: c
14:32
HR.S 	
HRS
hRS

HRS

HRS
HRS
H^S
«?.s
hRS
H.RS
8: £ r"*S

-
-^
~
^
yf.
•si
=;
12: a
14:32

7:15
15:15


12:15
2C:15
hRS
H-;S

H.RS
HRS


HRS
HXS
143.00 HRS
A V E S A"
148.90 HRS
152.90 HRS
155.30 HRS
A V = R A
14S.CC i-P:S
A V E R A

148.90 HRS
152.90 HRS
155. 20 >-?s
A V E S i
I*.1:. SO *-^S
152.^0 rSS
155.30 HRS
A V E R A
152.50 'rSS
A '] = R A
i-'-3.CO HsS
156. CO HRS
A V ERA

153. CO HRS
iil.CO HRS
TOT
R A
K 2
tET)
G E :
SET)
(ET!
(ET!
G E :
(£T)
G £ :

«£T)
(2T)
C E :

; £- )
(ET)
(ET!
G E :
(£T)
?£T)
C, E :
C£T>
G E :

(ET)
iET)
A L :
T F. :
S GENERATOR /SUL
H2 CCNC- INLET GAS
\-Z CCNC INLET GAS
1-2 CCNC CUTLET EAS
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
F2 CCNC CUTLET GAS
N2 CCNC INLET GAS
N2 CCNC IKLET CAS

N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
.":2 CCVC CL7LET GiS
.'<2 C~-v" CUTL-T GJS

H2S CCNC CL'TLST GAS
H2S CCKC CUTLET CAS
F2S CCKC CUTLET GAS
H2S CCNC CUTLET GAS
r20 CCNC CUTLET G.'-S
5-20 CCKC CUTLET GiS
H20 CC.'-C CUTLET GAS
H2Q CCKC CUTLET GAS
N2 IN:LET VCL FLCH RATE
"2 INLET VCL FLCr. P.ATE
N2 INLET VCL FLC'« RATE

WEIGHT CYCLCNE CLST
V.rlGHT CYCLCNE CL-ST
V.EI3HT CYCLCNH ELST
WEIGHT CYCLCNE DLST
FUR S
?GS-1CC! /
iGS-ICO! /
(GS-1C6) /
{GS-108! /
«GS-10S) /
(GS-1GS) /
(GS-iCO) /
i
•^
--
^,
; •;

-------
                                                               C A
                                                                              I  \VENTORY
                                                                                                                                    PAGE
                                                                                                   HCPPER
U>
OS
o

;:
1C :is K.RS ]'. • ,,-n (.?<; ipT)
li:15 r'.S 159. 'JO >-?$ t")
• V c ? »- c -
" R E5IC
« :-.£S r.
UAL s CN CARS:?
•J.'L s c;-; c>?.=:f
UAL s c-i C"^;:
!CS- 9C / Z=C!1,T) =
scs- -"C / Z'.cii.r; =
•:cs- ?c / ;•:'.•::. ,T 5 =
CCS- 9C / A:-;:a =
3. SCO
4.iiO
4.c£v
« ! 'A E I G H T )
S 1 V> EIGHT)
"S (XSIGHT)
1 !V<3IGhT;


':'•
•'-
>•
.'•



i'i
| ii . i i—

^5
u.
r"

F*1 '

LJ


_... 10:;? H?.S isi.-f! HR« (-T)
14:15 HR5 15K.CC HRS (ET)
18: 15 H».S 15S.CO !-RS <£T)
t v S " i G t :
7:15 r-RS 14S.C.O t-%3 !37)
15:15 f~.S 156. CO !-».S i£7)
AVERAGE:


1C:!5 H?.S 151. CO H3S !ET!
14:15 V-RS 155. CO HRS (£T)
15:15 S^S 156. CO r=.S itT!
20:20 H.RS 161.10 HRS IcT)
0:15 HRS 165. CG HRS (ET)
3:15 MRS 168.00 HRS tET)
T n -r ^ i .
1 Si I A t. '
RATE:
•



™ R5SIC
Z RESIC
L'AL H2C CN CA^fCv
UAL H2C CN Ci5.;C«
S RESiDUiL H2C CN C4SfC:\
3  / LI <1 i ft 1 —
C S-4CU / RS4C1 =




2.230
2.230
2.230
2.2ZC
71 ' ' "-
31. COO
31.000


0.0
3.700
13.300
4.200
5.CCC
3. CCO
2.024




? HEIGHT)
? ISEIGHT)
t i. -EIGHT)
LE iv^T'L/HR
L3 J-'AT'u/HR
LS XAT'L/rR


L3 SULFUR
LE SLLFUS
L2 SULFUR
LS SULFUR
LS SL'L'UR
L3 SULFUR
1 Q ' ' i[ CMO
LS SULFUS/HR




:




•:
s



i
—


!
-
-.
r. :
b* i.
a4
ita' " :*
ET r-
c :
3*. * ~-
L-
\tf
1*2 - -:
D
1 :

-------
ON
j
STATUS REPORT CF OPERATING CCNCITICNS FCR
r-: OPERATING PERIOD:
>: CATE: */2c/7A TlCt CF RECCRC: 7:1= H!
.1
•- PRCCESS ELAPSEC TK'c CF PERIOD: START 14 =

r-.
'»' SUXyiRY CF INTEGRATED PRCCESS PERFCRKANCE:
* 1. S02 RHyCVIL P-RSG2 =
•
ir 2. H2S UTILIZATION Pl)h2S =
'=.; 3. ACID CGNVESSICri (TO SULFUR) PVCS =
':i 4. 1-2 UTILHATICN 1 TC H2S ) PhCi-S =

;•« 5. SULFUR RECOVERY PRS
'f.'
t-. 6. V-2 UTILIZATION A" UNIT PU'S-2 =

W 7. RESIDUAL SULFUR CN CARSON X90A =
!_ j '
fc- 8. CASECN RECYCLE RAT= (CE! RC90 =
1 .
t 9. ACIO LCACIK-- INLET CARSCN 6" U.MT xsoic =
y
i« 1C. MOISTURE CCKTEKT INLET CARBCN 6" UNIT X301B =
to'
H 11. ACID LCiDING ISLET CARECN 8" UNIT X302C =
U 12. KOISTURS CC'.TE\T INLET CA^aC?>: £" UMT X302B =.
I;
a 13. TOTAL AC'" CC\VFRTFD S» UMT • PVC

jc; 1«. SULFUR CCNVcSSICN (TO H2S) PSCt-S =
C 15. SULfUR CCNCENSER EFFICIENCY £RV4CO«

n
• ; MATS FV=\TS CURING" CFERATING PERIOC:
Li 	 "
CUT CN C02 TD 40 CFH IN 4" UMT AND
'J REDUCED N2 TC 66 CFh AT 148.1 MRS.
U ATTEMPT TO TURN STEAM CN TO 4" UNI.I...AI ..
IXJ 150.3 !-*S. UNSUCCESSFUL DUb IU LKUlU.H^iO IN
\J 	 STEAV LIME. ELEX SULFUR FRCV RfcCl^UULAI Ii-.^
4/26/7A PAG; 7
INTEGRATED OPERATION CF S02 RECCVERV PRCCESS ,
i
S TC 15:15 HRS

.r'-i VR<; / p\n i?&.co HRS LENGTH CF PERIOD: e.oo FRS .,
i
:t
56.03 ? (ACTUAL) 9C.O ? (GCAL) '>

57.80 Z (ACTUAL! "55. C 31 (GCAL)
il.99 % (ACTUAL) ??.C t (GCAL)
iC.90 ? (ACTUAL) 90.0 3 (GCAL)
-
33.34 * (ACTUAL) 1CC.O S (GCAL) OF SCRBED S02
3C.75 3 {ACTUAL 3 25. C S (GCAL) CF STRIPPED SULFUR
ICC. CO S
;;
C.C467 LB S/LB C ::
T.
2E.957 LS C:C£I/HR W
C.2637 LB ACID/US C
:,-
C.C916 LE H2C/LB C
W
C.2637 LB ACID/LE C
C.C926 L3 h2C/LS C :,
t-;
64.17 % -i
z*
72.87 % -.
113.32 2 ;
.,
;.,
<;
t ;
„
r
PCT TG CVERFLCV. ?Ct 	 "' 	 ^

-------
                                                                                   4/26/74




STATUS REPORT CF OPERATING  CCNCIT1CNS FCP-  INTEGRATED CPER4TICN CF S02 RECCVCRV PROCESS
                                                                                                PAGE   S
r. 	
I •
ll
';
!«•
i1'
OPERATING PERIOD:
CATE: 4/26/74 TIME OF RECCRC: 7:

PRCCESS ELAPSEC TIPc CF PERIOD: START
15 fR5 TC

1'P

.:c HRS
15:15

/ END
HRS

15

6~.CC~


HRS


:
./
1.ENGTH CF PERICC: 8.00 t-RS
..i ~ 	 • • " 	 ,,
i.'
i ]
SULFUR MATERIAL BSLiNCE (USIN'G PROCESS H2S):







t
"> •>
•i
S 0 2

S C R B
E R





f •:
i/
i
•i

1»
LO T.
O"» si
10 U
- *
I N
INLET GAS AS S02
IMLET C AS RESIDUAL S
T C T A L IN:

CUT
CUTLET GAS AS SD2
CUTLET CARBCN '
CYCLCNE rUSI
COLLECTCR DUST
CiRBCX hEEPAGE
TCTAL CUT:
6" CIA C A R B 0
I (-
JRV-


£ C-
( [)-
(Ch-
(R'l-
l\
13) /
11) /
1C) /


13) /
12) /
ill /
12) /
12) /
1C) /
P R £
BG10A
SC11A
sue


BG13A
3C12*
BDlii
S012A
BCW12A
S010
C C N
3
=


=
•=
^
S
•=
t- I
2.
.1.
•3 ^


0.
3.
0.
0.
c.
3.
„ ,
3852
35 it
7363

CI20
0
C249
9740
C N
LE
LB
LS


L°
LB
LB
LB
LE
LB
<- 1.
SCLFUR/I-R <
SULFUR/hR
SULFUR/1-R


SULF'JR/KS
SLLFUR/HR -,-.
SULrUS/r-S -
SULFJR/HR -,-.
SULF'JR/l-R :,
SULFUR /!-.R ;,

W ;j
3» 7 N t'
i»
b
y
U

JS
3*'
rs
INLcT CARSON
T C T A C IN:
CUT
CUTLET CAR3CN
CYCLCVE CUST
TCTAL OUT:
S U L F U
( C-
(RV-
t C-
{ ;-
12) /
3:0 /
2 C ljL_/_
(RV-3CC) /
R
3 e N
BC12i
SI300
8C201A
BD30iA
S030C
e R A
=
=
=
=
=
T C
^ .
3.
3.
C.
3.
R
8444
3444
3444
0
8444

LB
LB
LE
LB
LS

SULFUR/hR -j
SULFUR/^R .
SULFUR/I-R ^
SULFUR/HR -.
SULFUR/hR :,
-
w •*•
!.-: IN
- -^ '.-•
1 - - 	 	 . -. i . - 	 	
•».fc

„
',*
, , 	
X
I'iLST GAS AS 1-2 S (CYL)
INLET GAS AS J-2S i?RCC)
'T C"T 4 L IN:

CUT
CUTLET GAS AS H2S
CUTLET GAS AS .S02
CUTLET CASF.CN
TCTAL OUT:
! G-
» »3"
! C-
1B\_
( G--
{ G-
! C
;nv-
2C1) /
2 C i ) /
2 C '' ; /
2CCi /


2C5) /
2C5) /
2C2) /
2 C C) /
EG201S
fc; = 03'',
GC201*
S;2CC


BG205B
"EG2Q5A
S02CQ
=
=


=
_
0.
** *
3.


0.
C.
7.
3.
C261
79 5S
6
-------
                                               	t_?_s_
   E R A T C R _/ J_ U  L  F L R
                                                                                                   STRIP
                                                                                                                £  R
                                      ! M
                                              INLET  CARBON
                                                 	T C T A
	( C-2C<)  /  BC202A
 IN:     (RV-icCJ  /   SIIOCT
_7_.9331__LE__SULFU3/I-R_
 7.~933i LB SULFUR/VR
                                     CUT
1 CUTLET
' CUTLET
j CUTLET
». CYCLCNE
» FILTER
f T
CAR8CN
GAS AS
GAS AS
CUST
C'JST
C T A L
H2S
s


OUT:
C-l
•3-1
0-1
C-l
[Rv-1
c: ) i
:4 > y
:i> /
C2) y
:o y
6C103A
8C1C4B
' 8G1C4S
BD101A
' 60102A
SO 100
=
=
?s
=
1
4
2
0
C
8
•
*
«
w
*
•
3516
0235
0
C
me
LE
LS
t a
L =
LE
LB
SU'LFUS/HR :
SULFUR/HR l
SULFUR/1-R
SU'LFU'R/hR
                                                          OVERALL
                                                                                 -  r U R
                                                                                            E A
                                                                                                      C E
OJ
*,
IN


t INLET GAS 13"

UMT AS

SC2

( G-- 1C) /
' INLET GiS 8" UNIT AS CYL V2S I G-2:i) /
* T 0 T A L S U J. = U R
= CUT
-•>' CUTLET
>•' CYCLCNE
* CCLLECT
:•- CiRECN
r CYCLCNE
s CU'TLET
CUTLET
» CUTLET
.: CUTLET
!i CYCLCNE
FILTER




GAS IB" UNIT AS
CUST "l8" UNIT
CR C'J£
CUST
GAS 8"
GAS S"
GAS 4"
GiS 4«
CUST
C'JST 4

T
6
4
It


SC2

IS" UNIT
IS" UMT
» UNIT
UMT AS
UMT AS
UNIT AS
UMT AS
" U.MT
IKU
T 0 T A
H2S
SC2
H2S
S
L

( G-- 13) /
( C- 111 /
{ D-- 12) /
(Cu- 12) /
( 0-3 CD /
( G-2C5) /
( G-2C5) /
t G-l :4i /
s G-I:-. ) /
: c- 1 : i ) /
S U L F ij R

8G10A =
BG2018 =
I N :

SG13A =
3DUA =
30124 =
8CVJ12A =
ED301A =
EG20J3 =
6G205A =
6G1042 =
3D 1C 1 1 =
'JD102* =
OUT:

2.
C.
2.

0.
0.
0.
c.
0.
c.
c.
c.
2 •.
c.
c.
2.
3852
0261
4112
094t
01 20
C
C249
C
1C61
3606
0
C235
0
6217
LB
LB
L3
~L2
LS
LE
L2
L2
La
"_L =
L2
LZ
LB
L5

SULFuR/KR
SULFUR/hR
SULFUR/t-R

SULFU'/I-R
SULFU3/rR
SULFLS/S-R
SULFU-R/I-R
SULFU'S/i-R
SULF'JS/i-R
SULF'JS/HR
SU-LFUR/.--R
SULFjP/'rS
S--FUS.'rR
SULFUS.'f-S
SU'LFU'R/hS


-
-


.5
t*
^
-.
—
w
-^

-------
HYCRCGEN MATERIAL BALANCE:
                                                                                                      PACE 10
i1;


j1.

M

I N
I
I
i
i




NLET.
•".'LET _
NLE7
:,LET
N.L.EJ




GAS AS
GAS AS
GAS AS
GAS AS
CASBGiV
.T C T

S U L f Li
•
H2
LJ 7 O f /* VI \
H2S (PRCC)
r2G
A L IN:

R .3

( <;-2:
I.- £. -
( r>2:
t c-2:
: c-2:
\ rv *" ' ^ 4

E N

3)../
3 ) y
u /
C) /

£ R A T C

BG2C3C =_
6G2C33 -
.BG203 =
BG203C =
8C201H =
J-I2CC =

S

C.
C.
0.
C.
C.
1



CO I 6
2997 "
3592
4505
mi

L ~
LE.
LS
LS
LE

.
HYCRCGEN/i-R
HYCRCGE\/!-R
HYCRCGEK/I-R
HVCRCG5K/HR
HYCsCGEN/SR 5

"CUT .

£«'
LJ
r
C
!.TL£T
•-•TLST
LTLET
OUTLET

T
GAS AJ j--2
GAS AS H2S
GAS AS I-2C
CAR5CN
C T A
,
L OUT:
( ; - 2 :
i (.-2j
! G- 2 :
( (.-2!
(RV-2-:
;} /
5 J /
5! /
2) /
Ci /
- f o '• = " —
EG205D =
SC202K =
HC20C =
C.
0.
0.
6 = 21
1632
3219
LE
LE
LE
LE
H^ciE^R ;
HYCRCGEN/l-R
HYCRCGEN/FR
J-!
r
73
-4
i»

w
t
rl
y

IN
I
CUT
C
C
C



NLEf "

UTLET
-TI-:T
LTLET
T
H 2 S

GAS AS
CA'RBCN"
T C T
CAS AS
GAS AS
GAS AS
CIA
G E N E R A T

l"2
ft L ! K :
H2
H2S
1-2C
L OUT:
n • r* '

v:- 1'.
{ C-2C

2997
2342
5339
?

L E
la
Lc
'?f
L 3
LS
E R -=

HYCRCGEM/KR -t
HYCRCGEN/HR rs
KVCRCGSM/t-R
HYCRCGE^/VR r>
HYCP.CGE;\'/i-R =
HYCRCGEN/1-R ••
» ^

-------
             APPENDIX A-12-11
EXPERIMENTAL DATA AND RESULTS FOR INTEGRAL
       RUN IR-2-8 (156 - 168 hours)
                     365

-------
                                                                                                                                    PAGE
                                     STATES REPCS.T CF OPERATING CCNCITIONS  FC:  INTEGRATED GPERATICN: CF SC2 RECCV'SY PROCESS
U)
'::
)3
\
•
,
y
;»'


-
>
F*
AT
'.j
'^
^
13

''--.
-
OPERATING PERICC:
CITE: 4/26/74



CATS: <./ 27/74

PRCCESS ELAPSE: TIME
*• . •
TTVZ re necCRC: 15:15 V'RS TC 24: C H^$ ;
TIME OF RECCRC: 'C: 0 >-R3 TC 3'-15 HRS



*
CF PERIOC: START 15i.CC HRS / ENC 16S.CO HRS LENGTH CF PERICC: 12.00 HRS
i
PROCESS VARIABLES FCR CPERATING PERICD:


•
18:15 HSS
22:15 HRS
2:15 HRS


IS: 15 HRS
22:15 HRS
2: 15 HRS


15: 15 HRS
3: 15 HRS
17:15 HRS



159. CO HRS (£T)
163. CO HRS !£T)
167.00 H?S SET)
AVERAGE:

15<3.CO HAS fET!
163.00 HIS (ET!
la 7. CO HRS 
16C.CO HSS (ET)
161.00 HRS (ET)
164. CO HRS (ET)
158. CO HRS 1ST)
AVERAGE:
'.61.00 HRS !tT>
163. CO H«S SET)
TOTAL :
RATE:
161.00 HRS !ET)
163.00 HSS (5T>
. . .0 .'. A.i- •
R i T E :
151. CO HRS -ET!
162. CO HS.S (ET)
168. CO HRS !£T>
C t £ L -
RATE:


S C 2 SCR
SC2 CCNC INLET FLLS G '-S
S02 CCNC INLET FLLE G !S
S02 CCNC INLET FLUE G »S
S02 CCNC INLET FLUE G !S

S02 CCNC CUTLET ?LLE >2S
SC2 CCIVC CUTLET FLUE >t$
*Q2 CCNC CUTLET FLUE J^S
SC2 CCNC CUTLET FLLE .J'S

H20 CCNC INLET FLUE G SS
H20 CCNC INLET FLUE G =S •
H20 CCNC INLET FLUE C SS
ORIFICE PRESSURE DRCF
CRIFICE PRESSURE DRC?
CRIFiCE PRESSURE CRCF
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
GRIP ICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
CRIFICE TEMPERATURE
ViCIGKT CYCLCNf CUST
hrlGHT CYCLCNE CUST
WEIGHT CYCLCNE CLST
V.SIGHT CYCLC.\c DUST
V.EIGHT CCLLECTCR DUSf
'.= IGHT CCLLECTC3 DUST
ucrrur rr; i PTTrR r^LSr
WEIGHT CCLLECTCS OUST
hEIGKT CARECN WEEPAG:
ii=IGHT C/.R8C.N KtEPAG:
wP'.'HT CAR3CN. KEEPAGr
vP'^-HT C*RSC\ KEcPASE.


3 E R
1GS- 1C! /
fGS- 1C) /
CGS- 1C) /
(GS- 1C) /

;GS- it) /

-------
20:15 t-".S
3:15 HRS
j-
=• 12:15 HRS
' 2C:15 HRS
3: 15 HRS
:
161. CO
168. CO
A V E
15 3. CO
1-61. CO
163.00
A V £
1-F.S
r'.S
a A
S--S
rSS
hP.S
S A
JET)
CETI
'o C 5
;ETI
t=Ti
tETl
G c :
S TCT
S TOT
S TCT
$ TCT
s TOT
? TCT
. s TCT
s
s
s
s
s
s
s
CN
CN
CN
CN

CVCLCN5 D-iT
CVCLCNE D'.V
CCLLECTCR
C.N CCLLSCTC3
CN
CN
CCLLECTCS
CCLLECTCR
I.ST
I:ST
UST
UST
{
{
!
{
{
(
{
D-
0-
D-
D-
C-
D-
0-
11)
11)
11)
12)
12!
12 J
12)
4/26/7*
            PAGE
ClliltT)
DlilliT)
AD11A
C12<1,T!
C12!1,T>
D 1 2 ( 1 1 T )
AD12«
S
=
=
f
s.
7
7
7
7
7
7
7
.760
.700
.700
.760
.640
.703"
3
«
*
{'.•EIGHTS
(V.EIGHT)
JV.EIGHT) ,
tfecICt-T) ::
(\;E!GhT! '••-
( * EIGHT) .<
(WEIGHT! -.

-------
                                                                                                                      A/26/74
                                                                                                                                 PAGE
     Ci
U>
cr>
CO
1
V
I


••'
i*. 	
f- -
fcr
S
I *",— 	 	 	
. r
' i
=:'
3

-..
*::
t.
y
id
£
-,
.-•
5*' '
U
1
"^
•fj
h ••


'•*'*
s.'
1
' _,


6" DIA CARBON PRECONCITICNER
14:15 HRS 155. CO MRS f ET ) S TOT S CN INLET CARIC\ (CS-301) / Z3C1U.T) =
22:15 hRS 163. CO KR3 ! ET> ? TQT S CN INLET ORiC\ (CS-301! / Z301(1,T) =
2:15 i-RS 167. CO US (ET! S TOT S CN IMLET CA?,!C\ (CS-3CU / Z30M1.T) =
AVERAGE: S TOT S CN INLET C1RICN (CS-3C1) / AZ3014 =

1<.:15 HRS 155. CO HRS (ET) ? H20 C.N INLET CARBC! • (CS-3C1I / Z30H2.T) =
22:15 HR5 163.00 !-RS ( = T) % (-20 CN INLET CARECI. JCS-3C1) / Z3C1(2,T) =
2:15 HRS 167. CO HR5 (ET! % >-20 ON INLET CAREG!. ICS-3C1I / Z30K2.T) =
AVERAGE: t H20 CN INLET CASED! CCS-3C1) / AZ301E =
2C:15 H^S 161. CO f-RS (ET! WEIGHT CYCLCNE CLST ( C-3C:j / C03C1(T) =
3-»C L.3Q 1AQ r f1 t-*1"! (i^Tl LrCTPi-T ^VPIfS^C f* t • C T f P- ->^*\ / rr'TOTfTX
T C T A L : WEIGHT CYCLCNE DUST I C-3C1) / WD3C1 =
RATE: WEIGHT CYCLCNE DLST ! 0-301) / RC301 =
15:15 I-RS 156. CO l-RS !ET) S TOT S CN CYCLCNE D'ST f C-ICH / C3C111.T) =
3:15 HRS 168.00 HSS (ET) % TOT S CN CYCLCNE J.ST ( C-3C1) / C3CHI.T) »
AVERAGE: Z TOT S CN CYCLCf.E 3.ST E C-3C1 ) / AC301A »











•

.






•

•
"
_ _
9.860 S (WEIGHT)
8.300 1 (VEIOS-TJ
8.060 S UEIGkT}
3.740 ? (WEIGHT)

7.0CO t (HEIGHT)
7.600 S UEIC-FT)
6.000 ? (VEIGHT)
6.867 S (HEIGHT)
0.0 LE CUST
*\> Cw l*w^l
C.O LS CUST
0.0 L8 CUST/kR
0.0 ? (HEIGHT)
0.0 * (V.EIGS7)
C.O ? (WEIGHT)





-
v




















'.
.
.
i;
•
„


•-

-
.
;
;
:
-
-
,
-
.
_
1
-
„
4
.
\
4
.
,

S
j


-------
                                                                                                                       4/24/74
                                                                                                                                    PAGE  4
U>
, ,. 23' ? HRS
16:20 H.RS
'.'• '• • 19: IS HRS

>»
20:26
21:38
HRS
HRS
23: 2 HRS

:•;
:~
'••:
•i

.
".
—
^


;,
-,
-,
— *


16:20
19: 15
20:26
21:3«
'

23: 2
16:20
19:15
20:26
21:38
23: 2


16:20
19: 15
21:36


HRS
HRS
HRS
HRS


HRS
HRS
HRS
HRS
HRS
HRS

HRS
H"
* C 1 5 **
*O _ . i V
A V S
	 j.57. iO
16C.CO
161.20
162.40
A V E
' 163. SO
A V E

157.10
16:, cc
isi.io
162.40
A V £

163.60
A y £
157.10
I6C.CO
161.20
162.40
A V E
163.80
_ A v_E

157.10
iiC.:o
161.20
162.40
HRS
HRS"
HRS
I-RS
R i
HRS
S A
HRS
HRS
HRS
R A

I-RS
R. A
HRS
HRS
VRS
HRS
R A
•-RS
n «

HRS
rRS
HRS
HRS
s.' A V E R A
3^
;
Ci'
^,-
j.
J3
.13
1 .
w
^.
^
'
.,
.,
^.
,"•

23: 2
15:13
3: 15


14:li
22:1?


14:15
18: 15
22:15
. 2:15.


14: 15
18: Is
? 2 : 1 S

J5. s.
HRS
HRS


HRS
HR S

".HRS
H^S

""•-.S
HiRS

162.KC
rt V' ""
:5t.co
156. CO
A V E

155. CO
ii3.c:
167. CO
A V E

1 e c /•/>
IP... 	
i?;!::
i V E
i '> "i • T «•
1=3. CC
>-RS
I> *
Hi-.S
_HRS
~R A

;--s
ur c
R. .A
HRS
HRS
_ : c
.-'• S
r •* i
!ET)
_( cT i
"lET>
IET)
(ET)
i E :
~G E~:

SET)
!cT5
lit)
G E :

(ET)
G E :
1ET!
SET)
SET)
(ET)
G E :
!ET!
G E :

(£7 )
SET)
SET)
_JST_) 	 	
G E ;
!ET)
G E :
(ET)
G E :

<=T)
G c :

(ST )
!ET!
s> c :

! nT )
11'. I
SULFUR GENE
SC2 CCNC CUTLET GAS
S02 CCNC CUTLET GAS
H2S CCNC INLET GAS
H2S CCNC INLET .G.' S
H2S CCNC. INLET GAS
H2S CCNC INLET GAS
H2S CCNC INLET GAS
H25 CCNC CUTLET GAS
H2S CCNC CUTLET GAS

H2 CONC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS
H2 CCNC INLET GAS

H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
H20 CCXC I^LET GAS
H20.CCNC INLET GAS
H20 CCNC INLET GAS
H2Q CCNC INLET GAS
H20 CCNC INLET GAS
H20 CCNC CUTLET GAS
H2C CCNC CUTLET GAS

N2 CCNC INLET GAS
N2 CCNC INLET GAS
N2 CCNC INLET GAS
"J2 CONC INLET GAS
N2 CONC INLET GAS

,N2 CONC CUTLET GAS
\2 CCNC CUTLET GiS
N2 INLET VCL FLC'.-. R.'<"£
Ni I;>iLcl VCL FLijV* RArc
N2 i'NLcT VCL FLC* Rii'-'E

I TCT S CN !\L£T CAsi'C-.
Z TCT S CN INLHT C-'.'. :C •.
i TCT S CN I.MtT C« "C.v
% TCT S Cr< INLET C*Ri'C.»

i5 TCT S CN CUTLET C.M e !N
% -7CT s c,\ CUTLET cA:.e:r.
Z 7^T S CN CUTLET C *> t :.\
'i TCT S CN CLT'.ET C .-::; :N
* TOT S CN CUTLET C'^e'.I.

i H2G C\ I '.LSi ^k?'!'~;
X, HiC CN :;-L£T CJr.d-
R A T C
IGS-2C6)
R
/ Y206\ltT) =
(GS-2CO! / Y2CCC2.T) =
SGS-2CC)
(GS-2CC)
(GS-2CO)
:2-T; ,
/ ZiSii^l! •
1.650
1.650
23.300
25.600
24.4CO
25.600
24.725
0.0
0.0

0.200
C.O
o.c
C.O
O.C50

0.0
0.0
22.400
24.100
23.400
23.300
23.300
49.600
49.600

56. COO
52.400
54.2CO
53.2CO
53.950

45.330
AS. 200
127.000
127.000
127. COC

9.S60
£.300
c.CiC
8.74?

20.500
IS. COO
Ic '.940
19.210
6. COC
!
1
S (VCLUME) )
? (VCLU«£) °j
? ! VCLUHE) J»:
1 (VCLUMEJ '•;
^
3
"s
2
3

?
?
?
•*
S
?
<
?
S
s
?
*'
,
(VCLUME) i;1
(VCLUME) .;
(VCLUME) .•!
(VCLUHE) :«i
(VCLUHE) • =

iVCLU.ME) -:
(VCLUKE) «
(VCLUVE)
(VCLUXE) '-i
! VCLUHE) ,1
:-y
(VCLUHE)
(VCLUME)
73
(VCLUWE) :•
(VCLUME) .-=
(VCLUME) ri
(VCLUME) _-;
(VCLUMEI ;,
(VCLUME) r
(VCLUHS)
_.
(VCLUME) ;,
(VCLUHE) :,
(VCLUKE) _•
(VCLUME) i,
(VCLUME) J
:s
(VCLUME) :.
S IVCLUKE) .-
CFH (70 DEG F) -.
CFH (7C CEG F) ^
CFH (70 DEG F)
5
•»
t.
t
rf.
(V.EIGHT)
(WEIGHT! .;
(XEICHT)
.
(HEIGHT! ^
ti.eiGH.ri j
(»5IOH7!
(WEIGHT)

'.'A SIGH 7)
(hEICHT)

-------
                           2:15
                                 h'.S
                          22: 15  -RS
  A V E  S  i  5 6  :

J55.CO  I--.S  (£Tj	
 155.CO  rSS'i'ET)
 153.:3  r3S  1ST)
_157.CO _(-?S_lST5
...X.'V .-  s  i  G E ^-_

J55.CO  HS"JET)~
 15?.co  i-=:s  JET;
 153.CG  r^S  IET}

~i V E~H~A~~5"'£  :
                                                              ?  f-ZC CN  IN'LET C/SS6CN
_S_H2D_C\  CUTLET
 S -r2C CN~CU7LET"CAR8t.\
 * -1-2C CN  CUTLET Cs3.SCv
_?_!-2C CN'  CUTLET C.'-
JS_*C I P_CN_CUTl. = T_C A R E : N
 S AC'i'C  CN CUTLET  '
                                                                                                iCS-302)  /     AZB025  =

                                                                                               JCS-200 )._/_:2CO ! 2, T 1 _=_

                                                                                                (CS-2CC!  .
 JCS-2CC>_ /_    iJ2CCE  =

JCS-2CC!_/_Z2CO!3,T)  =_
 1C S-2C C 1" /" Z 2C 0 ! 3, T )" =
 SCS-2CC)  /  I20Ci3,T)  =
 'CS-2CC?  /  ZiCCiB.T)  =
                                 6.867

                                 3.100 ?
                                "3.2CC ?
                                 2.7CC ?
                                                                                                                                         (*>EICHT>
                                                                                                                               _       _         _
                                                                                                                                3.500 3  i ȣ!GrT)_
                                                                                                                                3.E2C ?  IVEIGt-T)
                                                                                                ICS-2CC)  /
                                                                                                               AZ200C =
                                  _
                                 3.S70
                                                                                                                                                 _
                                                                                                                                         (VvciG'rT)
OO
•>J
o
        w
        L,r

-------
                                                                                                                       4/26/74
                                                                                                                                   PAGE
                                                  H  2  S
                                                           GENERATOR/!. JLFUR
                                                                                               STRIPPER
                      17:15 HR
                                                       H2  CCNC INLET GAS
CO
16:20 H9S
19: 15 H1RS
20:24 HRS
21:38 HRS
17:15 HRS


16:20 r-?S
19:15 HkS
2C:2t HRS
£ !.- 2. >i r"^ S
0:15 HRS
1:15 rR S
3:15 HRS
16:20 HRS
19:15 HRS
20:2i HRS
3 i * "3 ;> ijO C
3: 15 HRS _


16:23 HRS
15:15 rRS
20:26 HIS
21:3= HRS
•0:15 -RS
1:15 HRS
3:15 HRS
15:15 H.R3
3:15 HRS


20:15 hRS
3:15 HRS


20:15 HRS
3:15 HRS

14:15 HRS
15:15 HRS
22: 15 rRS
2:15 HRS
AVERAGE:'
157. 10 HRS (ET!
16C.CO H'RS !£T)
161. 2C HSS (ET!
162.40 HRS 1£T)
AVERAGE :
153.00 H"
TOTAL:
RATE:

161.00 HRS iET)
153. CO HRS (ET)
TOTAL:
RATE;

155.00 HRS (5T>
15S.CO H:'.S (ET)
16!. CO HRS !JT)
167. CO HSS tET)
!-2 CCNC INLET GAS
H2 CC\C CUTLST G4S
H2 CCNC CUTLET GAS •
H2 CCNC CUTLET GAS •
H2 CCNC CUTLET GAS
H2 CCNC CUTLET GAS
N2 CCNC I.NLET GAS
N2 CCNC INLET GAS

N2 CCNC CUTLET GAS
NZ CCNC CUTLET GAS
N2 CCNC CUTLET CAS
M2 CCK.C CUTLHT GAS
\!2 CCNC CUTLET GAS
N2 CONC CUTLET GAS
N2 CONC CUTLET GAS
N2 CCNC CUTLET GAS
H2S CCNC CUTLET GAS
H2S CCNC CUTLET EAS
I-2S CCNC CUTLET GAS
t-?^ (" f* N: *~ f" ! ' T 1 P T f* fi %.
H2S CC.NC CUTLET CAS
H23 CCNC CUTLET GAS
H2S CCNC C'JTLET GAS
H2.S CCNC. CUTLET GAS _.

H2C CCNC CUTLET G&S
H2C CCNC CwTLET GAS
H2C CC.NC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CUTLET GAS
H20 CCNC CL'TLET GAS
N2 INLET VCL FLCX RAT£
•;2 INILET VCL FLCV- RATE
iN2 INLST VCL FLCV. RATE

SvEIGHT CYCLCNE CLST
HEIGHT CYCI.CNE CLST
V.EIGHT CYCLCNE CLST
WEIGHT CYCLCNE CLST

WEIGHT FILTER CUST
WEIGHT FILTER CLST
WEIGHT FILTER CUST
HEIGHT FILTER CUST

3 TOT S CN CYCLCNc CLST
% TCT s CN CYCLCNS OLST
2 TC" S CN CYCLCNE CL£"
% TOT S CN CYCLCNE CLS'
«CS-iCOi /
tGS-lCE) /
iGS-icaj- /
SGS-1CS! /
C'G S"~ I G £ ) /
CGS-1CC! /
JGS-1CC) /

CGS-106! /
(GS-1CS! /
C'C-S-IOS) /
JGS-10S) /
(GS-103! /
(GS-10S) /
(GS-10E) /
(GS-10E! /
rGS-lOE) /
iGs-ioai /
fi^C 1^31 /
I3S-1CE) /
(GS-iO£! /
JGS-108! /
(GS-lCe! /

(GS-1021 /
iGS-lCE) /
JGS-iCc! /
•GS-ioa; /
(GS-10e) /
(GS-103) /
SGS-ioe: /
1SS-1C ! /
( G-1C ) /
! S-1C ) /
: c-ic ) /

< C-IC ) /
1 C-IC ) /
! 2-10 ! /
t C-1G ! /

5 D-1C2) /
{ 0-102) /
J 0-1C2! /
5 C-102) /

I C- 1 C 1 ) /
< C-ICi) /
c c-ioi ;• /
t o-io: ) /
YiC£!2." )
Y1C6(3,T !
YlGSJ2tT)
Y1CS!3,T !
AY10SC
Y10DI5.T!
AY1CCE

Y103(5,T)
YlC3(r, T)
V1CS ! 5,T;
Y i06 \ 5 1 i 1
Y108i5,Ti
Y1C3(5,T)
Y1GS(5,T)
AYlOcc
Y1C3;2,T!
Y1CS(2,T)
Y1C8(2,TJ
Vl^S*1? f * "
T i-.j O t £ s I /
Y10S!2,T)
Y108(2,T)
AY108B

YJ03 ( 4, T I
Y^I i^'I1
Y103 (4 , T )
YiC8x4,T)
Y1C3 ! 4, T )
AY10SC
Gioois.n
GiCO! 5,T}
AG100E

ccioi in
CClCIiT)
V.'DIOI
SE1G1

CDI021T)
CCi02(7)
RD1C2

C101 11 ,T)
C1C 1(1,7)
C1C1U.T •
= 4E.500 ' ;VCL'JVE)
C.2GC S SVCLUXE)
0.0 S t VCLUME)
= 0.0 J ! VCL-JKE)
C.O ? (VCLUME)
C.050 ? (VCLUME)
51.500 S (VCLUME)
51.500 S (VCL'J."£)

56. COO ! (VCLC^E)
52.400 ? (VCLUX.E!
= 54.200 S (VCLL'ME)
53.2CO ? (VCLUMS1 .
52.50C ? !VCLUHE)
= 54.100 ? t VCLUME)
52.600 t (VCLUME)
53.571 ? (VCLU.Vc)
23.300 (VCLUME)
•= 25.600 (VC4.lJC.EJ
24.4CO t VCLUME)
— 1 ^ i.^^ ' /\'f"ll!>^Cl
= 26.100 ;VCLU;-;E)
= 24.100 (VCLUKE)
. 26.100 (VCLUME1
*> 25.029 (VCLUCE)

22.400 (VCLUKEJ
24. ICO (VCLLJKEJ
23.4GC- S ! VCLUME)
= 23.300 % (VCLUME)
= 21.000 * (VCLUKE)
= 21-400 % (VCLUME!
21.000 ? (VCLUHE)
22.371 S (VCLUME)
127. OCO C?H (7C C=G F)
127.000 CFH (70 CEG F)
= 127.000 CFH (70 CEG F)

0.0 L8 CUST
0.0 12 CUST
C.O LS CUST
C.O IS CUST/HR

O.C LS CUST
= G.O LE CUST
= 0.0 LS CUST
O.C LE CUST/HR

» 4.t6C S (VcIGH.T)
4.t2C % (WEIGHT)
= 4.;~0 ? («=IGHT) ;
4.220 ? ('.EIGHT)
:
.
j

i
a
-:
-:
4
-J
-,
-7
-,
»
_
--

-t
~f
f 3
^'
it
•:«
S*'
-:>
_,
_.
.,
-
^
--
jj
3
.-
,-
._
;'

-------
                                                                                                                                      PAGE

                                                        I TCT S  CN  CYCLCXE CLST         ( D-lCl)  /    A315XA »       A.490  S  (hEIGHT)
                                                        JLJCT_JS_?1_?1»J5
-------
                                                                                                                              4/26/7*.
                                                                                                                                           PAGE
U>
~J
CJ
14-.ll
13:15
22:15
2:15


14:15
13:15
: 22:15
2:15

H.RS
HRS
HRS
h?5_
HRS"
HRS
hRS
HRJ

155. CO
159. CO
16 2. CO
157. CO
t V E
" 155.00
159. CC
163. CO
167. CO
A V E
hRS
t-=!S
r-, S
R. -
f-RS
l-RS
..r * S
"* A
(ET)
(ET!
G £ :

"IET")
«ET1
IET!
S E :'
C A R 8 C N i ^ V
3 R=S!D'JAL s CN c*.'.ec:\
* >e$!Cu*'L s CN c^secs
S RESIDUAL S CN CAR3C;\

S RtSlCUAL H2C ON CARSC!-
* RESIDUAL H2C CN CJRHLM.
% RESI3U4L H2C CN CiRcUi
t S-SiCU'L H2C CN CiR2'>

E N' T C R Y
(CS- 90) /
CCS- 90) /
;cs- ^c:- /
!CS- 9C) /



15:15
3:15
HRS
HRS
156.CO
lfc3.CC
A V t
HRS
•r'r.*
R A
t JT )
G~S :
CA^ECN RECYCLE RATE
CA33CN RECYCLE RATE
CiRSC\ RECYCLE RATE
( C- 90; /
! C- 90) .'
i C- 90 > /
C9D 1 1 » t i
C90'. 1,T !
=
IT
=
31.000
31.000
31. COO
IS
LE
LE
MAT'L/i-R ^
t'AT'L/HR !«
•f
•»
.




SULFUR CO
N C E N S 2 ft




-•
i
1C:15
14:15
15: 15
2C:15
. C : 1 5
3-- 15
-
hRS
hRS
HRS

hRS
HRS

15;. CO
155. CO
156.00
161. CO
165. CO
163. CO
T
•-'•'S
I-'.S
h^S
i-P.S
G T
iET)
;ETI
SET)
!ET!
!ET»
i L :
T E :
•-.SIGi-T SULFUR CCLLECT;-.
*EIGriT SULFUR CCLLECT=":
V.HIGI-T SULFUR CCLLECTE:
V

-------
                                     STATUS REPCRT OF  OPERATING  CONDITIONS FCR INTEGRATES OPERATION Cf SC2 RECOVERY  PROCESS
CO

'
OPERATING PERIOD:
C6TE: 4/24/74 TIME CF RECCRC:
CATF: 4/27/74 TIX= 2F RFCCRC:
15:15 H
AS TC 24". 0 HRS

0: 0 h^S TO 3=15 HRS
.:

PROCESS ELAPSED TIKE CF PERIOD:
START 156
.CC hRS / END 166. CO rRS LENGTH CF PERICD: 12.00 hRS
SUHVARY CF INTEGRATED PROCESS PERFCRCANCE:

••,

1. S02 RE.-CVAL

PRSC2 «

95.14 ? (ACTUAL) 90. C 31 (GCAL)
..
t
•3

•- •:'
'':•
r.
--


•~
2. r2S UTILIZATION
3. AC 10 CCNVERSICN I TO SULFUR)

4. (-2 LTILIZATICN ( TC H2S)

5. SULFUR RECOVERY
6. (-2 UTILIZATION V U'HT
PU!-2S *
PVCS =

PHCl-S -

PRS
PU!-2 =
ICC. CO S (ACTUAL! 95. C ? (GOAL)
63.69 % ? ACTUAL! 99. C 5 (GCAL)

62.46 * (ACTUAL) SC.C S (GCAL)

88.08 % (ACTUAL) 1CC.C S (GOAL) CF SCR3EC SC2
33. 2C ?. (ACTUAL! 2S.C S (GCAL) OF STRIFPEC SULFUR
c c . g 3 5;
;
.»
•
«
70
~
.3 ~>
..


*,
-c
-
'^
1 	
i.
.-
i

7. RESICUAL SULFUS ON CAReCN
3. CAR5CN RECYCLE RATE (DB)
?. ACID LCACING I\L=T CARECN 6" UNIT

1C. XCMSTURE CONTENT INLET CAR3CN 6" UNIT
11. ACID LCACUiC- INLET C«ECN 81: Ur: I T
b2. ."Q! STL-RE CONTENT T.NLET CARBON 8" UNIT

13. TOTAL JCIC CONVERTED 8" UNIT
1*. SULFLR CC^VE?3iC^f 1 "C- *2S S
i?. iLiFLS CCN--ENSER EFFICIENCY

X9CA =
RC90 *>
X3C1C =

X301S =
X3C2C =
X3023 =

PVC =
PSCi-S =
ERViCG =

C.C431 LS S/LE C
Zfi.917 LB C«DE5/HS
C.2159 LB ACIC/L3 C

C.C932 L3 P2C/LE C
C .215S L3 iCI:/LE C
C.C932 LB H.2C/L3 C
.
75.96 S
SC.7C Z
172.04 S



•*

.,
-_-,
77
i,'

-
-

_..

fijCR EVENTS DURING OPERATING PERICC:
f'j- c"? cc2 TC •»•' u>;r~ :
-------
                                STATUS SzPCRT CF OPERATING CCNCITKNS PCS INTEGRATED GPER2TIC.X C? SC2 RECCVERY PROCESS
CO
OPERATING PERIOD:
futfi 4/2t/?4 TIVE QF RECCRC: 15:
CATE: 4/27/74 T;*E Of RECCRC: o-.

PRCteSS SLAPSEC TlYE CF PERICD: START
SULFUR MATERIAL BALANCE (USING PROCESS h2S):


S 0 2
I N
INLET GAS AS S32
INLET C AS PESIDUAL S
T C T A L IN:

CUT
CUTLET GAS AS SC2
CUTLET CiRSOi
CYCLCKE CUST
CCLLECTCR OUST
CtReCfv V,EE?AG£
TCTAL CUT:
6" OiA CAR30

I N
I.NLET CAR3CN
TCTAL IN:
CUT
OUTLET CAR6CN-
CYCLCNS CUST
TCTAL OUT:
S U L F U

I N
INLST GiS AS I-2S (CYL)
!.\LET GAS AS r2S (PftCC)
INLET CiR3CfJ
T C T A I IN:

CUT
CLTLET GiS i.5 H2S
CUTL3T US ii SC2
CUTLET C-3.-,CN
T C T i L OUT:
15 HRS
0 HRS

156. CC
-


S C :
( G- 13)
( C- 11)
IRV- 1C)

t G- 13)
( C- 12)
i c- in
( C- 12)
(CV,- 12)
!RV- 1C)
N P


I C- 12)
(RV-3CC)

< C-2C1)
< C-3C1)
(RV-3CC)
R G E


( G-2C1)
( G-2C1)
( C-2C1!
(RV-2CC)


! G-2C5!
i ** ~ r ^ i
! o — i C:> }
! C-2CZ)
IRV-2CC)
fC 24: 0
,'C 3U5

;RS / EN'S



( 8 E R
/ 3G1CA
/ sen*
/ s:io

/ SG13*
/ OCI2*
/ eon A
/ 3012A
/ 3CK12A
/ S010
J c C C N


/ 3C12A
/ SI3CC

/ .SC201 A
/ SC3G1A
/ SC30G
S = R a


/ EG 201=
/ KG2G3R
/ SC2C14
/ SI20C


/ 2G2C52
/ SC202.3
/ SOZOC

HR

i
*




=
S
X

=
—
=
=•
=

c


=

=
=

T C


:
=


S
S
-

S

68. CO




2.
1.
3.

0.
2 m
0.
C.
c.
3.
I T I


3.
3.

•5 ^
C.
3.
R


C.
3.
e.


c.
7.
7.



I-RS




,1.*
3919
£065

1173
cos;
0
0039
5543
C H


4301
4301

4301
C
4201



A
9 ise
3439


0
-6 .; 5
3703








L5
Lc
LE

Lc
IS
LE
LE
LE
E R


L2
LB

LS
LE
L6



te
L c
1 ^
LE


!_ C
1 C
I 2
LE



LENGTH CF PERICC: 12. CO HRS




SULFUR/H*
SL.'L.CUR/HR
SLLfUX/HR

SULFUR/hR
SL.LFUR/I-R
SULFUR/l-R
SULFUR/f-R
SULFUS/HP.
SULFUR/hR



SvLrUR/1-R
SULFUR/HR

SULFUR/t-R
S'uLFUR/hR
SULFUR/HS



SLLFUR/l-R
SLLFuR/i R
SULFCR/1-R
SULfUR/t-ft


SULF'J^/f-R
S^L?UR/tp
S^Lr-JR/r-K
^i i
.' j
';
-,:

'3
,-l

;;
•B-
T.
rj
73'
-2

M 5
^ i
.,
>,•
^
;j
TJ .
=-,
C^
	 1 1
is


^
.' 1
_^
i
' 1
.,
-'
'.,

-------
*3:
'•

•
i!
,
a:
K
s .
; j
•?
r;

ft
t:
-:-

pj
»
!,.•
! •
>" - 	 i
; N
r:' ET cisscN
T C T 4 L IN:

CUT
CUTLET CiRBCN
OUTLET GAS AS 1-2S
CUTLET GAS iS S.
CYCLCNc uUST
FILTER CUST
TOTAL OUT:
OVERALL

I .N
INLET GAS IS" UNIT AS SC2
INLET GAS 8" UNIT AS CVL H2S
TOTAL
CUT,
CU'TLET GAS 18" LNIT AS SC2.
CYCLCNE CUST 18" LNIT
COLLECTOR CUST 13" UNIT
CARBCN XEEPAGE 13" UNIT
CYCLONE CUST 6" UNIT
CUTLET GAS 8" UNIT AS H2S
OUTLET GAS 8" UN.IT AS SC2
CUTLET GAS 4" UNIT AS H2S
CUTLET GAS 4" UNIT AS S
,C'YCLC\E CUST 4* UNIT
FILTER CUST 4" LNIT
T G T A L S
t C-2C2)
tp.\-:cc>


t C.-1C4!
I — iv 1 )
( 1-1C2)
!R>-1CC)
S L L F U


< G- I C J
t C-2C1)
S U L f U

( G- 13)
< !> ; 1 )
r C- 1.2)
fc;-.- J2>
1. G-2C5J
( G-2C5)
! G-1C4)
I G-1C4)
/ ,"_ 1 '• T J
( C-H2!
U_ L'F I! R

/ SI10C =


/ BC1C3A =
/ BGLO^S =
c 01 C i /i ~
/ b0102A =
/ SC100 =
R B A L A


/ SG10A =
/ 6G201E =
R IN:

/ BG13A =
/ B011A =
/ ED12A =
/ 8D3C1A =
/ BC-2058 =
/ EG2C5A =
/ BG1CAS =
/ EG1C4S =
/ 3D1C1A =
/ 3D102A =
GUT:
7.
7.


1.
2.
.
C.
3.
.N C


2.
C.
2.

C.
0.
C.
c.
c.
G »
c.
c.
2.
C.
c.
2 •
4569
4369


391?
C235
C
3342
^


4146
C

1173
CC55
0
CC39
0
C
3S35
n
0235
0
C
5337
* T?
L £


Lc
LS
L3
L c
IE
LE



LE
LS
LS

LS
LB
L2
LE
LE
LE
i a
LE
LE
IS
La
La
SULFU'R/rfi
SLLFuR/:-R


S^LFUR/hR
SULFUP./HR
SUL rUr\/!-K
SULFUR/f-R
SULrUR/HR



SULFUR/HR
SULFUR/HR
SULFUR/t-R

SULFUR/HR
SULFUR/HR
SULF'JR/i-R
SL'LFU'R/i-R
SULFuR/J-R
SU'LFUR/V-R
SULFUS/rR
SULFUR/l-R
SLL?ljR/t-R
SLLFUS/hR
S'-UFUR/f-R
SULFUR/I-R
•
.
:
•
r
•T
-r
>
-,.1

•
»
-

-<
-•;

-:
" :

-^

-------
                                                                                             <./26/74
                                                                                                         PAGE  12
HYORCGE^ fATESIAL  BALANCE:
                                    SULFUR     CEKERATCR
r N



!' TNI FT r,A<; i* H?
•' INLET (
;\LcT !
•' INLET :
•i •
i.
•- CUT
CUTLET
^' CUTLET
'-•' CUTLET
T
"*
r.
'- - IK __
K INLST
k- INLET
1
t CUT
':-. OUTLET
i- •—— • CUTLET
S>.' CUTLET
;ASJ
"• A c
&AS ,
T C


GA5
GAS
r AS
iS 1
iS I
S.S i
-2S (CYL)
K2S ;PRCC
r-20
T A L I


AS
AS
AS


HZ
H2S
1-20
CARS ON
r T

M 2
GAS"
A

S
AS"
L C U

GEN

h2
CAP-SCN
T C
GAS
GAS
GAS
T
AS
AS
AS
A L I
H2
H2S
i-2C


< G-SC:

:> < G-5
' ! G-2
< C-2



{ G-;
< G-2
( C-2
T : {RV-2

E R A T C R /

.;t

Ci

:
( G-1C
( C-2
N : 1RV-J
! G-i
« G-l
t G-;
r
/• |
u
if-
\f'
c-

1) / SC203C »
I) / BG'035 =
!> / EG203C =
:> / (-i2cc =


i) / B0225C =
i) / 2C205:- =
:} / 2C275C =
.') / BC202:- =
.-) / S-C20C =

; u L F u R

5) / EG103C =
21 / 8C2C2H »
:> / moo =
;•! / BG10AC =
t) / aciC4h_»
Vi / EG104C »

C.
0.
0.
c.
r*
i.


0»
0.
0.
o *
0.

S T S

0.
c.
0.
0.
c.
0.
coot
o..
2S41
4 2 ~ "
CI£9


7203
ISlV
I P
4921
IS 14
6735
C036
2074
2747 "
LE
LS
ii
L'S
L E
L c
1 c
L£
P
LE
L2
LE
LE
LE
LE

HYCRCGEN/HR
HYCRCGEN'/H^
hVCRCG£'!/i-R
HYC?,CGE\/rx


HYCRCGcM/Hft
i-YCRCicN'/rS
HVCSCG:.N/(-R

c R

HYCRCGEN/1-S
HYCRCGEN/fR
HYCSCGEX/l-R
HYC^CGEH/HR
HYC?.CGE\/rR
i-.YCSCGE.N'/S-R
,.
-

1


-

3

"I
»
-,
;;
r<
.H
.
^
i>
                     TCTAL
                                  CUT:
                                                 /  t-cicc =
                                                                       0.5S27 L£ HYCRCG=N/hR

-------
              APPENDIX A-13





DATA FROM SOLVENT EXTRACTION EXPERIMENTS
                  378

-------
u>
I

>70_7-

i

033-71 J


i
j
F
•
|































r££9 212
t"-:ii)?S 20- ao

:r.e 1 5 "-'n. contact i

Water ".'."ash
' 1\
v J-/
(2)

Boiled.' EgO^ & Cried































1
20. ±5z
•
\
C ~V~



i



C'-activ:























i





i
14.01S


siurrv


3.72^-S
c.6

p, £ rlc

Ltv ret-a




















i
i
•
;
•
i







--•'tat1
	 	 i






-ir.ed 26




















:



t

t
I




lOOnl

.on







&
































































i
i










^0 Tiin


8.^S
.8.3

1-1 \
o. 4

























'


1






. corrbad





































;
]
I

t 60 ~-'r

'
i S.5-1S


; D -
I
i
j
!

1
1
j

,


!
;
i
;

__ 1

i
i












i


i


















-





















,4.






























j
|

t
\



















































1
!
i


1



.
i
i



;



•


,





i





                                                                                         CTJfi ~"
                                                                                         ~A

-------
to
00
O
	


i
306-3^6 C-TO^TfVirzir. carton 1 '


3C6:; : 31






3063 : ',1


306o:46


3065:^5
























i
i







0.5-3


30g l
















i - i


-.0?

j


4-0 g
j



'
iOg

t
i








I
1

!




i




































	 : j
:








	 _






CSp

50rJL
1 extn

i
j
1
	 	 — 	 "1 	 	



30 ITT'




fTJfi, )nQ]
4 "-
""OOrJ.




i. agitJ














Inert '. Degassed.
C-as •
i j
j
•
(air) !

CSlfOT"^


No
"
! I!
} :
1


10 aii. 'aeit.
|

>•-„-£








i
fair) ii So
1 extn lii!
i i
~6?ri
1. soak

~TOnl


30 nit. soakj_ t Heliu-' ;:o.


60 rai]







t















I i
! 1

i. soak












' S t & ?,TTl9 CL



<
:

1 No











IP ^-',1
1 !>


t

; i







i
; T7o i i • ^- C''~


' 1.5 ~^-

i
Ro

1300 CF

' 1}
60 mic

— .

-200° J
's^ow exhaust s
3
J £ far.

! S ^0 C"1

250-
T5°F

['
t
1 -L. « . C
tear
I


:

! 1 . : ";-3
1
1
! i !
i: ' : • '••














i
i
;
• • '
:









:


; i

ii
i M
i i '
;

I i • i
' j i i !
i :

> t;
:i i .
i ' ' • i

•\
I ,


: ' ' i i '
!
; ; j
]
i

' ' -~~*^-


'. i
i




1 :


;
j
j-
i

1
i
i
1
i
ii
i !i ; |i ;
1
1 1! ;l
: 1 ! t < i

*
; | .
1
i
i!
t ,
                                                                        RiSEARCH C:

-------


--7Q-77















OJ
nr.
I-1












•










-

FEB9-212 i
Xyler.e

1 Sxtrn.

2

-3

1.

c;





Carbon used


*-i

7

Q
-
9

10




1







i

23s

ol-i'-UOt
0.6^5^

3.4^'.-



^  ' i '
j ! i !
i ' '
; i ; i !
' -• i
' \ i

) 1
t t
i : -; 	
' I
; i
1
; i
i ' 1
i
! ' t
! 1
; , |
1 ! ! i
'- \ \
I ; !
CHARLES ic:; ?iSD-\Rc:-:

-------
	 1-

3-70-77











ZZS:.' 312 21.4s
352




14.0-^3
j
{
1

( 5Ctol
{ i "Ro r> r*>-<-

;l

1 ictrn. : 3.~?.~ -^.?±
00
K •*












'

'
6

T


i 45ml
! i

0.97g



3.12
i
3 1
1

o

10




0.6le 2.56

15.62




3-2?iS




[Under














-





1
Sxtrn .


Air

slurrv





77CF
aeitat]

Decanted
Solvent

Solvent





re -freshed
45

45ral

45

45.0

45nl




.on. ~£0



i
i
evapd. 4 r^toe^ OD 105


i



!
041571





o . i6gS^

0.08lg

0.054gS

O.OSOg

O.O^e

O.OllgS




min.




°C o'ni

















y








": -— - - ; 	 | --

; •
!
1
; . 1
!

> \
| :

.
i
! 1 :
.



\ \


|




!
; i
i

: '
! i 1
' : 1
r i I i








I



!
i i


i i


i
i
|
i



t

1


















i
i



j
J
























i
!
1

:
i
! i
3' - . -i i '

:





i

	
•
'


! i
3068 3 45 ; •;

i
1

t
L !
!
!

,


j
I !



1
)


!
i
! i


i


I
CHARLESTON i^

-------
oo
U)


C-70-77
.









































IES9-312
(!5T.iI)o5 15£aq

1 Sxtrn.

2

q



39 -2g


O.p5-g




l^.OfcS i^~65cc)


ti . ^OvSS

0.6-1
6.96

0 . ^?P

4 ' lC.5~D

q


5.33.








4.96

0.5--5 ~.l5

6 b. 556 ^.5o

7

R



0.536 3-^

0.51?

q .'•. 0.5c2

10

Wash & Steamed

















0.7^5

27.226?


Under
Extrr..

^.16

2.80

2.72

2 . 08^5


Kp
100-1C
C"l rC'LL

HpOvas'd 100-1


Stea-ied





^ t---ss


















5°F
ating

05C?

j
256-2E
c cr.




• 051171
' "-^ T~ C* • G **1
i -< ' 7> S o-9
0°P










(lOCtal
Reco

70nl

iO

35

75

80

dO

85

85

92

120ml





^5ccpir


60ccptr


70ccp:r.









1.012K1
vered

l-35gS

1.28

1.05

0.77

0.68

0.595

0.52=

0.510




^)


'















0.486

0-587





25rnin.














i
i













I






|



•





!

;




1
: i '
* 1






















i !







..
i
i


i













1



1
i








s










i '

•
1
!







i



i
:




































































i
1 |













































                                                               CKARLE3TC":  .IE3EARCH OEMIi.

-------
CO
oo
•P-
                                                           CEARLESTOM  3SSEAHCE CE.TEE

-------
CO
OO
•^•HMB^HMm..!!!.!!!.
C-70-77












, • • ~ .





., " .-_\ '•••' ' '





















. ' ' i '
5SS9 KL2
(EHk)oS 15%aa

1 Shcfcrn.

2

3 ;-.-.

k

5
-, ,, - .
Washed & Steamed










.









•






WOIMBVBIIVI»-lll«^H^H
tO-9s


1.099K

^VP^H^P^H^I^^^^^
l^O^S


io.6i*&

l-.l66c 17.48

l.Wws

1.29k?

_

^0.277s


Under

JJjctra. -


BfcsO wa
~ 3 t

Steased
8 hr


J^rbon












?.W3^

6.76*

_

U;08%


H«


circxala

h
E3S (~3





Act!










042971
^175 I 1-k

(~65cc'

















K)5tF
tine

105° F
0 mln.e

25O-275



itv Re-















(100ml
Reco

75iaL

85ml

80

80

130ml






35ccpm

;-"
a)60ccp

"F
70ccpn


ained 4















3.4823:3
vered

l.tesS

1.26g

0.96g

O.Tle

0.92K3






30 mln


c
-




T.h%















»)










r















































^,_
— -
























3Q.7g


L.637K

1.6o6s

JL.696g

L-455R

_

?9-033


As P


temr:


it.o^a


10.00^;

8.^2

7-52^

6.2%

_

2.80^


brjj


L avay
i
i



















3175 S
hot cv

















Ct2371


(~6SCG


1
5













except


got t<
,le per:


















1-2 i




Hecc

SOml

QCfel

90

80

135TTJ.




during


1000°3
od 1/2























vered

l.sfigS,,

1.33s

1.07s

0.935e

0.93gS




steamin



- 3/4 h



















1


!
I








1
1



f
•







e l

i

t




















•








1





                                                         CHARLESTON iSSSARCH CENTER

-------
oo
ON
                                                              CHARLESTCIT :S3SARCK  CEi.TZ"-:

-------
00


C-70-77








































j

—",-•,—. — — j~*
~ ~~-~^ *-* .""- t*_
CT-iOoS 204 ac |

1 Sirtrrs.

CL

•J

h

5


Lp.29a


2.03^

2.Coe

2.60s

2.35s

-

Washed Sc Dried i3C.5"'2







"





















Under

Sxtract


Water v

.Decante

Car"bon













3,053 S
lii.o^c


10-O^S

5.284

5.14-

4.8^

-

k.k%



Air

jd slura


ished bi

1 and o

ictiviti












0319T1
32





















y agits


• slum

ren drie

• retail

















lOCfcl

















,ted




:d 105° d

ied



































15 min




ovei niJ

20. E$


































.




zht















































































1


























!
1 !








.

















































































1 !
•
i
I











1


1









1

!








[


t
i

















































1
! 1 i


1













                                                                  CHARLESTCII  SESZAHC.I C7LIIT7

-------
                            APPENDIX A-14
           LITERATURE SURVEY  FOR RECOVERY OF SULFUR
                       BY  SOLVENT EXTRACTION
I.   SULFUR RECOVERY -  REVIEW ITEMS
     1.   Berthelot, Ch. Recovery of sulfur in the coke plants in Germany.
             Genie Civil 113, pp. ^01-6 (1938).

     2.   Berthelot, Ch. Recovery of sulfur in coal-carbonization plants
             and petroleum refineries.  Genie Civil  116, pp. 6-7 (19^0).

     3.   Brabant, M. Desulfurization of (town) gas and sulfur recovery
             processes.  J. usines Gaz 6k, pp. 33-^3, ^9-56, 69-75 (19*4-0).

     k.   Brabant, M.  Desulfurization of gas and processes for recovery of
             sulfur.  Schweiz. Ver. Gas-u. Wasserfach.  Monats-Bull. 21, pp
             26-30, Ul-2, 96-100,
     5-  Bulian, W.; Dittmar, A., and Feher,  F.  Removing elementary sulfur
            from natural gas.  Erdoel Kohle, Erdgas, Petrochem. 20 (12),
            pp. 849-52 (1967).

     6.  Evans, E. C. et al-Special study of  sulfur removal and recovery
            from fuels.  J. Inst. Fuel 29, pp.  138-9 (1956) .

    *7«  Goar, B. G.  Today s sulfur recovery processes.  Hydrocarbon Process.
            1968, U7(9), PP. 2^8-52.

     8.  Grosskinsky, 0.  Recovery and utilization of nitrogen and sulfur pro-
            duced in coal carbonization.  Bergbau - Arch. 5/6, pp. 1^6-52
            (19^7) .

    *9.  Kronacher, H. K.  Modern Desulfurization Processes in Germany.
            Gas-Age Record 68, (2), pp. 37-56 (1931)-
 * Filed in Charleston Research Center
       Translated into English

                                  388

-------
 10.  Lissner, A.  The importance of the sulfur of coal in the German
         raw-material economy.  Tech. Niederdonau 1, 197-9, 218-21
*11.  Lorenzen, G.  Purification of Gases with Special Attention to
         Desulfurization and the Recovery of Sulfur.  Chem. Fabrik
         12(1,2) :6-23 (1939).
 12.  Muhlert, F.  Recovery of by-product nitrogen and sulfur in the
         coke-oven and gas industries.  Brennstoff-Chem., 10, pp. 1*87-
         90 (1929).

*13.  Powell, Alfred R.  Recovery of  sulfur from fuel gases.  Ind. Eng.
         Chem. 31, PP- 789-96 (1939)-

  14.  Rosendahl, F.   Recovery of coke-oven gas products.   Oel u. Kohle
           ver. Petroleum, 36, pp.  229-^3 (19^0).

  15.  Secchi, I. M.   Recovery of sulfur from coke-oven gases.  Chim.
           e industria (Italy) 19,  187-91 (1937).

 *l6.  Sweeney, E. L.  and Sands, A.  E.  The removal of free sulfur
           from spent oxide.   Gas Age - Record 779  pp. 657-62 (1936).

  17.  Thau A.  Extraction and utilization of fuel-gas sulfur.  Z. Ver.
           deut.  Ing.,  Beiheft Folge 1938, no. 3, pp. 8l-6.

  18.  Wagner, P.  Utilization of spent oxide from gas works.  Rev.
           Prod.  Ghim.,.2U, pp.  397-^ (1921).
                                 389

-------
II.   SOLVENTS  FOR SULFUR EXTRACTION

      A.   Ammonium Compounds

              1.   Aoki, T.; Morikawa, M. and Akiyama, Y. to Sumitomo Chem.
                     Co.  Recovery of sulfur from hydrogen sulfide.  Japan
                     patent 582,626.  April 12, 1958.

              2.   Collin, F. J. A-G.  Extraction of sulfur from fumes con-
                     taining hydrogen sulfide.  British patent 7^8,037-
                     April 18, 1956.

              3.   Gluud, W., Schonfelder, R. and Riese, ₯. Purification of
                     sulfur from gas plants.  Brennstoff-Chem. 8, pp. 168-9
                     (1927).

              ^-   I. G- Farbenind. A-G.  Gas purification.  British patent
                     320,190.  Aug. 25, 1928.

              5.   Pieters, H. A. J.  Removal of hydrogen sulfide from gases.
                     Brennstoff-Chem. 18, 373-6 (1937).
             6.  Wallis, E.  Recovery of sulfur in a marketable form from
                     flue gases.  Brit. Chem. Eng. 7, pp.  833-6 (1962).

             7.  Williams, P. E.  Treatment of spent oxide.  British patent
                     596.  Jan. 9, 1909.

      B.   Aliphatic Hydrocarbons and Derivatives

             1.  Alexander Wacker Gesellschaft fur electrochemische Industrie
                     G.m.b.H.  Recovering sulfur from used gas-purifying
                     masses.  Brit, patent 508,966.  July 7, 1939.

             2.  Bonner, L. C.  Treating gas purifier.  British patent 10,780.
                     May 1,
              3.   Every, R. L.  and Grimsley, R. L. to Continental Oil Co. Pre
                     paring  dispersable  sulfur.  U. S. patent 3,318,666.-

              k.   Genther  et  Franke.  Extraction  of sulfur.  French patent
                     377,82*1.  May 15, 1907-
                                  390

-------
            5.   Muszkat,  K.   Production  of free  sulfur  from hydrogen  sul-
                    fide-absorbing materials  in  the Warsaw Gas Works.  Gas  i
                    Woda 17,  pp.  235-8  (1937).

            6.   Roga,  B.   Gas purification masses  as  a  source for the re-
                    covery of sulfur.  Przeglad  Gorniczo-Hutniczy 30, pp.
                    i+32-6 (1938).

            7.   Simpson,  C. H.  Extraction of sulfur  from  material contain-
                    ing elemental sulfur.   U. S. patent 3,063,817.  Nov. 13,
                    1962.

            8.   Stobe, R.   Reclaiming sulfur  from  the mass  used for gas
                    purification.   German  patent 708,031.   June 5,
C.   Aromatic Solvents
            1.   Anon.  Recovery of the  sulfur  from spent oxide.  Gas World
                    57,  197 (1912).

            2.   Becigneul,  J.   Obtaining sulfur from gas-purifying materials,
                    U. S. patent 833,573.   (1907).

           *3.  Bradley, G. W. and Barritt, D.  T.   Sulfur.   British  patent
                    72^,119.  Feb. 16, 1955.

            k.  Germogenova, E. V.  Utilization of  mixed  solvents  for the
                    extraction of sulfur from sulfur  ores.   Mineral.   Syr'e
                    1937, no. 5, pp. 28-35.

            5.  Herold, P.  to I. G.  Farbenind.   A.-G.   Purifying coke-oven
                    gases,  etc.  German patent  570, M*8.   Sept.  26, 1928,

            6.  Hunt, E. J. and Glidden, W. T.   Recovering sulfur  from
                    tarry spent oxide.  U. S. patent  105,996-   April 29,
                    1913.

            7.  Jaeger, A.   Sulfur extraction from spent  gas-purification
                    using tetralin (and low temp,  tar oils).  Brennstoff
                    Chem. 3, p. 356 (1922).
                                  391

-------
         8.  Katewinkle, R.  Recovery of sulfur from spent oxide by
                 means of tetralin.  Brennstoff Chem.  3, PP«  310-1
                 (1922).

         9.  Kuster, 0. R. to Lummus Co.  Continuous counter current
                 crystallization.  U. S. patent 3,337,30?. Aug. 22,
                 1967.

       *10.  Prchlik, J. ; Hlinak, L. and Kartakova, C. D.  Recovery of
                 sulfur from spent gas works purification mass.   Paliva
                 3U, PP. 298-305 (195*0.

        11.  Rosen, R. to Standard Oil Dev. Co. Removal and recovery of
                 free sulfur from gas -purification materials, etc.  U.
                 S. patent 2,195,870.

        12.  Soc. d Eclairage, Chauffage et Force Matrice. Removing
                 sulfur and nitrogen from exhausted gas-purifying mass-
                 es.  French patent
        13.  Suru, J.  The desulfurization of gases.  Technikai Kurir 8,
                 pp. 31-2 (1937).
        1^.  Weil, J. A.  to Imperial Industries Ltd.  Sulfur.   British
                 patent 561,370.   May 17, 19^.

        15.  Wohlwill, M. to Metallgesellschaft Akt.-Ges.   Reclaiming
                 sulfur from gases.   German patent 707,132.  May 15,
D.  Organic Sulfur Compounds

         1.  Anderson, W.   Cyanogen compounds;  sulfur.   British patent
                 127,128.   June 15, 1918.

         2.  Capell, R. G.; Wright, J.  H.  and Cruse,  Wm. A.  to Gulf Re-
               •  search and Dev. Co. Recovery  of elemental sulfur from
                 sulfur-bearing solid mineral matter,  u.  S. patent
                 2,897,065.  July 28, 1959-
                               392

-------
         3.   Chemische Fabrik Phonix, Rohleder and Co.  Recovery of
                 sulfur from extracts of gas-purifying masses.   German
                 patent 182,820.  Nov. 16, 1905.

         k.   Deal, Carl H. and Papadopoulos, M. N. to Shell Oil Co.   Re-
                 moval of sulfur-containing gases from gaseous  mixtures.
                 U. S. patent 3,363,989.  Jan. 16, 1968.

        *5.   Potsdamer, L. S.  Notes on sodium prussiate.   J.  Ind.  Eng.
                 Chem., 11, pp.  769-70 (1919).

         6.   Strauss, F.  to Gottfried Bischoff K.-G.  Extraction of
                 sulfur-containing materials.  German patent 1,1^7,566.
                 Apr. 25, 1963.

         7.   Strauss, F. to Gottfried Bischoff K.-G.   Recovery  of sulfur
                 from gas purification masses. German patent 1,131,192.
                 June lU, 1962.

E.  Other Organic Solvents

         1.   Johnson, E. J.  A theory of fluidization and  its applica-
                 tion to sulfur recovery by solvent extraction.   Inst.
                 Gas Engrs. Publication no. 378 (a),  39 pp.  (1950).

        2.  Murphy, E. J. Removal of sulfur from spent oxide.   J. Gas Lighting
                136, pp. 396, pp. 396-7 (1916).

        3.  Sawa, M.. to Nittetsu Mining Co., Ltd.  Crystallization of sulfur in
                solvent refining.  Japan patent 6318,207.   Sept. lk, 1963.
                                    393

-------
III.   USE  OF ACTIVE  CARBON IN  SULFUR  RECOVERY FROM GASES

       1.  Bakes, W. E.; King, J. G. and Sinnat,  F.  S.   Sulfur  compounds  in
               water gas and their removal.   Dept.  Sci.  Ind. Research, Fuel Re-
               search, Tech. Paper 31, 35 pp. (1931).

       2.  Braeuer, H. ₯.; Rogge, K.  Natural gas refining  by desulfurization
               with active charcoal.  Erdoel, Erdgas Z.  1967, 83(5), PP-  170-8.

       3.  Brychta, M.  Separation of sulfur from Lurgi  generator gas.  Paliva
               36, pp. 391-9 (1956).

       k.  Carbonisation et charbons actifs.  Desulfurizing gases.  British
               patent k79,klO.  Feb. k, 1938.

       5.  Englehardt, A.  Use of active materials  at coke  ovens and gasworks.
               Glukauf 73, pp. 925-33 (1937).

      * 6.  Fischer, F. and Kloeckner, L.  New method for the purification of
               viscose exhaust air.   Wasser, Luft Betr.  10(12), pp. 833-5 (1966).

      * 7.  Grantham, L. F.; Larsen,  C. M. to N.   American Rockwell Corp.  Sulfur
               production from flue gases.  U. S. patent 3,^38,733.

       8.  Griffiths, H. Activated carbons-modern applications for adsorptive
               processes.  Chem.  Trade J. 96, pp.  235-6  (1935).

       9-  Hoffman, Th.  New methods and goals in desulfurizing illuminating gas.
               Chem. App. l6, 6l-63, 120-1 (1929).

      10.  Rollings, H. and Evans, E. V.  Report  on  removal of  sulfur compounds
               from town gas down to 10 grains per 100 cubic feet.  Institute of
               Gas Engrs. Pub. no. 1^6/^3, 21 pp.  (1936).

      11.  Knauf, G.  Application of activated carbon for sulfur removal  in gas
               purification.  Energietechnik 1968,  17 (ll), pp. 14-85-8.
                                   394

-------
*(T)12.  Koenigstuhl, M. D.  Extraction of sulfur from the hydrogen sulfide
             of coke-oven and other gases by means of activated charcoal.
             Coke and Chem. (U.S.S.R.) 1932, no. 7, pp. 32-7.

    13-  Kostrikov, V. I.; Keltsey, N. V., and Nivin, P. I,  Use of one
             sorbent to remove both hydrogen sulfide and carbon disulfide
             from rayon-industry waste gases.  Khim. Volokna 1968(2).

    l4.  Krczil, F.  Catalytic oxidation of hydrogen sulfide in presence of
             active carbon.  Chem.-Ztg. 6l, pp. 2*4-7-8, 2^9, 267-8, 269-70
             (1937).

    15.  Metallgesellschaft A-G.  Removal of hydrogen sulfide from gas mix-
             tures.  French patent 1,388,^53.  Feb. 5, 1965.

    16.  Weuwirth, F.  Desulfurization of gas with Koflach lignite charcoal.
             Berg-u.  Huttenmann.  Jahrb., 76, pp. 1-13(1928).

    17.  Stanisz, Z.  Regeneration of sulfur from gases by means of activated
             charcoal.  Przeglad Chem. 2, pp. 530-1 (1938).

    18.  Thoma, M. Fine purification of gas.  Schweiz, Ver. Gas-u.  Wasserfach.,
             Monats-Bull.  16, pp. 257-68(1936).

    19.  Todd, E. W.  Removal of sulfur from illuminating gas by activated
             carbon.  Nova Scotian Inst. Sci., 17, Pt. 2, pp. 12-3 (1928).

    20.  Visconti, Y. S.  Obtaining elementary sulfur.  Rev. brasil. guim.
             (Sao Paulo) 22, pp. ^15-18(19^6).

*(T)21.  Waeser, B.  Desulfurizing gases.  Chem.-Ztg. 52, pp.. 617-8, 638-Uo,
             658-9 (1928).
                                    395

-------
IV.   SOLVENT EXTRACTION OF SULFUR FROM CARBON

      A.  Ammonium Sulfide

             *1.   Comm. on Gas Mfg.  of the  Assoc. Technique.  Gas purification
                      by activated carbon and  recovery of sulfur in the solid
                      form.  Gas Journal, 184, pp.  526-7 (1928).

          *(T)2.   Egorov, N.  N., et al. Purification of gases with activated
                      carbon.   Chapter IV,  pp. 37-47 of "Removal of Sulfur
                      from Coke-Oven and Other Fuel Gases," Moscow, 1950.

          *(T)3.   Engelhardt, A.  The use of active charcoal in the gas in-
                      dustry.   Gas-u. Wasserfach 71, pp. 290-7 (1928).

              4.   Evans, K.;  Pearson, H. P., and Reisemann, E. Industrial
                      Applications of Active Carbon.  Trans. Inst. Chem. Eng.,
                      Dec. 6,  1929, pp. 62-83.

              5.   Gouthiere and Co., and Ducanel, P.  Recovery of sulfur from
                      used gas-purifying masses.  Ger. Patent 245,570.  July 14,
                      1910.

              6.   Kazarnovskii, S. and Pisarev,  K.  The purification of gases
                      from hydrogen sulfide by oxidation on activated charcoal.
                      J. Chem. Ind.  (Moscow) 12,  pp. 913-21 (1931).

              7.   Prchlik, J.   Removal of active carbon of sulfur from waste
                      gases obtained during production of town gas in the Lurgi
                      generator.  Prace Ustavu Vyzkum Paliv 1963(6), pp. 138-50.

              8.   Reichert, 0. and Stemmler, H.  to  Spinnfaser Akt.-Ges.  Recovery
                      of sulfur from activated filter charcoal.  Ger. patent
                      1,054,655.  April 9,  1959-

          *(T)9.   Spechal, W.   Sulfur removal from  synthesis blue gas by active
                      charcoal.  Gas-u-Wasserfach 94, pp. 679-8U  (1953).

             10.   Szilagyi, I.  Method to purify and to remove sulfur from  the
                      raw gases produced.from lignite.  Magyar Kern.  Lapja  4,
                      pp. 24-5 (19^9)-
                                       396

-------
       11.  Tyulyukov, A. and Khronova, M.  The purification ol' gasen con-
                taining hydrogen sulfide by active charcoal.  J. Chem.
                Ind. (u.S.S.R.) 12, pp. 2^7-5^ (1935).

       12.  Zel'venskii, Ya. D. and Volkov, A. E.  Gas purification from
                hydrogen sulfide by oxidation on active carbon.  Trudy
                Gosudarst. Nauch.-Issledovatel.  i Proekt. Inst. Azot.
                Prom. 1952, no. 1, pp. 131-8 (1953).

B.  Organic Solvents

        1.  Becigneul,  J. J. M.  Extracting sulfur from spent gas-
                purifying materials.   Brit, patent 9»800.

       *2.  Braeuer, H.  W. and Fischer, F.   Recovery of carbon disulfide
                with simultaneous removal of hydrogen sulfide.   DECHEMA
                monograph 1968, 59(10^5-1069),  173-89.

        3.  Brychta, M.   Desulfurizing coke-oven  gas by activated carbon.
                Prace Ustavu Vyzkum Palio 1962(U), pp.  169-232.

        U.  Cornillaux.   Extracting and purifying sulfur.   French patent
                353,932, March 25,  1905.

       *5.  Fischer, F.  and Kloecker,  L. to Pintsch Bamag  A.-G.  Process
                of regenerating activated carbon  saturated with hydrogen
                sulfide and an organic solvent present in  exhaust air or
                oxygen-containing gases.  German  patent 1,259»8U5,
                Feb. 1,  1968.

       *6.  Riedl, R.;  Brychta, M., and Praskova, D.  Regeneration  of spent
                activated charcoal used for the adsorption of hydrogen
                sulfide from pressure  gas by toluene and xylene. Sv.
                Vyspke  Skoly Chem.-Technol. Praze, Oddil Fak. Technol.
                Paliv Vody 3, no. 1,  5-3^ (1959).

       *7.  Schreiber,  F.  Use of tetralin in sulfur recovery from active
                charcoal used for gas  purification.  Brennstoff-Ohem., 3,
                PP. 355-6 (1922).
                                  397

-------
                       APPENDIX A-15
        S02 ACTIVITY AND PORE VOLUME DETERMINATION
                OF SOLVENT EXTRACTED CARBON
                                                        Page

1.   S02 Activity of Solvent Extracted Carbon            399

2.   Surface Area and Pore Volume Distribution of        420
      Solvent Extracted Carbon
                            398

-------
            APPENDIX A-15-1



S02 ACTIVITY OF SOLVENT EXTRACTED CARBON
               399

-------
GRAVIMETRIC   PLOW   EXPERIMENTS
RUJI:
Dry Weight:
Dol'lnction:
Carbon :
3 2' Mi
<>'j. 'i2 me.
2t
• > ' "',: -
2000 ppm
EXV-1
NO:
02:
H20:
t:

0 pt>m
6p
200° F

FL:
                                                       3500 c-c/min.
                                                       76.66
                                           Correction:  0.5007
                                           Date:       March 23, 1971
Time
minutes
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
32
•A
:tf
•!H
40
42
44
46
liff
r>0
52
54
56
58
(,0
>'<'>
70
Load
nig. HaSOl|/g. C
6.57
8.86
10.63
11-99
13-34
14.80
16.26
17.83
19 . 50
21.37
23.04
24.92
26.64
28.67
30.65
32.74
34.82
• 36.80
38.99
41.18
43.27
45.45
47.96
50.25
52.65
54.94
57.44
60.05
f.2.55
65.05
f.9.85
75.06
79.86
Ml). 97
»')-VV
<)4.'*7
]00.t>8
10'l.lM
110.51
115.1-2
120 . 52
125. 7 S
JSO.M4
lv'..05
l4l.2»
15^.2'-
]..',. 24
Mean Load
tng. HgSOii/g. C
if
6
8
10
12
lit
16
18
20
25
30
35
4o
45
50
55
60
65
70
75
80
85
90
95
100
110
120.
130
i4o
150
160
170
180
190
200
220
21+0
260
280
300
320
3!tO
360
380



Rate
mg. %30^/g. C/min.
4.3520
3-5446
2.4395
1.6681
1.3553
1.4283
1.5325
1.6264
1.7098
1.8766
1.9912 '
2.0955
2.1789
2.2623
2.3249
2.387^
2.4291
2.4708
2.5021
2.5334
2.5542
2.5751
2.5959 '
2.6063
2.6063
2.6063
2.6063
2.5959
2.5646
2 . 5229
2.4917
2.4500
2,'WK
2.335-1
2.2621
2.1268
1.9808
1.8140
1.6785
1.5221
1.3866
1.2198
1.0530
0.8862



                        400

-------
                GRAVIMETRIC   FLOW   EXPERIMENTS
(CONTINUED FROM PREVIOUS  PAGE)
Run:
Dry Weight:
Deflection:
S02:
Carbon:
129- G
95-92 nig.
-2.53 rag.
2000 ppni
EXV-1
NO:
02:
H20:
t:
0 ppm
3-5$
ft
200° F
Ft:          1500 cc/min.
$ HgSO^:     76.66
Correction:  0.5007
Date:        March 23,  1971
Time
minutes
75
80
85
90
95
100
io(;
110
115
120
125
130
135
ikO
11*5
150
155
160
165
170
175
180
185
190
195
200
205
2.10
215
220
Load
nig. HgSOij/g. C
177.33
188.70
200.17
211.53
222 . 58
21'«.11
2k 1 . 12
252.92
26.1.78
270.5l|
278.77
286.80
291*. in
301.1*0
308.38
315.16
321.52
327.88
33^.2U
3'*0.60
3't6.61t
352.90
35«.53
361). 16
369.58
37^.90
VfH.W
.VM.W
Wf.'jl
391-37
                                         401

-------
GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
130-0
101.7U mg.
-2.55 mg.
2000 ppm
EXB-1
HO:    0 ppm
02:    3-5*
HgO:   6%
t:     200°F
                                                        1500 cc/min.
                                                        76.66
                                           Correction:   0.5019
                                           Date:        March 2k, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
30
12
ll)
16
18
20
22
2U
26
28
30
35
l»o
1*5
50
55
60
65
70
75
80
85
90
9';
300
110
120
330
3 >(0
350
160
170
180
390
KOO
. 210
220
2'jO
«l|0
,"'.>0
i'M
."70
280
'f III
•iuo
110
:«o
H'J
Ixsad
m«. H2SOl,/g. C
5.11
5.90
6.39
6.88
7-37
7.76
8.16
8.li5
8.85
9.2't
9-93
10.52
11.21
11.89
32.68
13.37
llt.3.5
Il4.8lt
15-73
16.51
18.58
20.71*
22.90
25.3.6
27.1*2
29-98
32. Ok
35-29
37.81*
110.59
1*3. Mt
'16.29
1*9.31*
52.29
58.1*8
6k. yr
71-95
79-12
86.30
93-28
100.65
108.12
115.1*9
122.76
129. 61|
136.52
I'l.-i.llO
]50.(M
.156.67
11,2.77
I6((.'i,,
17li.5t,
lllu. ',i,
J»5.77
J'M .17
Tlh.2!)
20.1 . 30
Mean Load
mg. H2SOl4/g. C
1|
6
8
10
32
3.1*
3.6
18
20
25
30
35
1*0
'•5
50
55
60
65
70 ,
75
80
85
90
9'J
100
110
120
130
l'*0
150
3.60
170
180
190
200






















Rate
rag. HgSOlj/fi. C/min.
. 3.M'><>3
0.5» 17
0.31(1)0
0.32!i'i
0.33'(2
O.Vi'tO
0.3M7
0.38.-M
o. 1*128
o. n5.2i
O.liyl'*
0.5 '308
0.5701
0.5<>9n
0.6291.
0.6'ib7
0.66?U
0.6t3o
O.i>,'7>)
0.7077
0.7175
0.7175
0.7273
0.7273
0.7273
0.7175
0.7077
0.^979
0. 66S.lt
0.6W?
0.6291
o.wv;
0.5/01
O.^liO'i
0.5011






















             402

-------
GRAVIMETRIC
Run:
Dry Weight :
Deflection :
S02:
Carton :
131- G
102.52 mg.
-2.1*5 rag.
2000 ppm
EXV-2B
NO:
02:
t:
0 ppm
3.5*
200* F
FLOW  EXPERIMENTS

                   *v
                                                      1500 oc/min.
                                          Correction:   0.1*851
                                          Date:        March 25, 1971
Time
minutes
1
2 •
3
1*
5
6
7
8
9
10
12
ll*
16
18
20
22
21*
26
28
30
35
1*0
1*5
50
55
60
65
70
75
80
85
90
95
100
110
120
330
Jl|0
150 •
.160
370
180
1^0
2
l.Y'l.70
183.38
.191.. 57
l<)<>.',7
207.76
;M',.57
2J2.98
230.10
2.16.H3
21*3.27
2l(9.)(l
255-56
261.1*1
266.68
Mean Load
mg. HgSOl^/i;. C
1*
6
8
10
12
ll*
16
18
20
25
30
35
1*0
1)5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
ll*0
150
160
170
180
190
200
220
21*0
260



















Rate
mi-. H2SOl|/r- C/rain.
7.5595
U.8771
1.7070
0.5365
0.5365
0.51162
0.5560
0.5657
0.5755
0.61U5
0,61*38
0.6730
0.7121
0.71*13
0.7603
0.8096
0.8369
0.;V,6l
p. «97l*
O.yi69
0.9H61*
0.9559 •
0.9-'5'7
0.9852
0.991*9
l.OlWt
1.02l(2
1.021*2
1.021(2
1.001*7
0.9751*
0.91*62
0.9071
0.668:
0.81911
0.7316
0.61(38
0.5'»62
















'


            403

-------
Run:
Dr.y W.'ir.ht.
C-it-l on:
101 .'/O mi1;.
-3.74 u\i'..
li'KX) ppm
KXB-2
                                     NO:
                                     II20:
0 ppm
V//,
r/
200°F
              1500 cc/niln.
              72,06
Corroi-tlon:  0.4706
Date:         March 30,  1971
Time
minutes
]
2
3
4
5
6
7
8
9
10
12
14
16
18
20
22
24
26
28
30
35
40
45
50
55
60
65
70
75
80
85
90
9'J
100
110
J20
no
I'lO
.1^0
JnO
.170
1 :•'.<>
I'KI
2OO
21'.)
220
230
240
2'jU
2'.0
2/0
i'.".0
Lofid
mg. IlgSO^A;. C
8.44
9-13
9.r>2
9.81
10.40
10.79
11.09
11.38
11.68
11-97
12.56
13-25
13.94
14.62
15.21
15.90
If.. 68
17-27
18.06
18.84
20.71
22.67
24.63
26.59
28.56
30.52
32.58
34.74
36.80
38.96
41.22
43-57
45.83
4;-i.i8
'-•!.. I')
',.'..-<>)
M.Y',1
f.('.2B
74 .'iM
:•;().:/,
'-<..'!'>
".;.i.'i
'i.'.'M
j ( <•* . •>;>
IC". "1
31',.U
IL'O.'K'
12... SO
i-'.j. •;•-••
ny.'>°.
J.4 -i . .J,^
r4.(.;'7
Mean Load
mg. H2SOj+/g. C
It
6
8
10
12
Ik
16
18
20
25
30
35
4o
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
lltO























Rate
mg. HgSO^/g. C/isin.
8.6850
5-6919
2.3553
0.3925
0.3435
0.3435
0.3435
0.3533
0.3631
0.3925
0.4220
o.44i6
0.1*612
0.4809
0.5005
0.5201
0.5299
0.5397
0.5^96
0.5594
0.5692
0.5790
0.5888
0.5888
0.5888
0.5888
0.5888
0.5790
0.5692























                                       404

-------
Run:
Dry Weight:
Deflection:
S02:
Carbon:
GRAVIMETRIC   FLOW   EXPERIMENTS

                   NO:
33't-G
99.98 mt;.
-2.83 my.
2000 ppm
EXV-2C
0 ppm
3.5?,

200° F
                                             Ft:
             1500 cc/min.
             7!*.77
Correction:  0.1*883
Date:        April 12, 1971
Time
minutes
1
2
3
l*
5
6
7
8
9
10
12
lit
16
18
20
25
30
35
1*0
U5 l
50
55
60
65
70
75
80
85
90
95
100
110
120
130
lUO
150
.160
170
JBO
190
200
2K)
2HO
230
2'tO
250
?/<0
270
280
200
300
Load
mr,. HgSO^/g. C
32.I|0
13. yo
l't.90
15.90
16.90
17.90
18.80
19.80
20.80
21.90
23.90
25.91
27-91
29.91
31-91
37.11
te.31
^7.71
53.01
58.61
61*. 31
70.11
76.02
81.92
88.02
93-92
99.82
105.92
111.92.
118.12
12l*.12
135-93
I't7.53
158.83
169.93
iHo.yi*
i<):i..6i*
20.1. 9'*
,2.11.9'*
221.5')
2 -|i ).8';,
2-tO.tf';
2'iM.lO
2'..(..'i')
Ht'Ji.lfi
272.05
27').jr,
2H5.06
2',«.66
209. l/,
30'). 26
                                     405
Mean Load
mg. HgSOtj/g. C
6
8
10
12
11*
16
18
20
25
30
35
1*0
i*5
50
55
60
65
70
75
80 '
85
90
95
100
. 110
120
130
ll*0
150
160
170
180
190
200
220
2l*0
260
280
300





'






Rate
mg. HgSO^/g. C/min.
12.2525
9.5019
6.7511)
3-1*507
1.1002
1.0002
0.9902
0.9902
1.0102
1.01*02
1.0602
1.0802
1.1002
1.3202
1.1302
1.1502
1.1602
1.1802
1.1902
1.2002
1.2002
1.2102
1.2102
1.2102
1.2102
1.2102
1.2002
1.1902
1.1602
1.11*02
1.1102
1.0902
1.0502
1.0202
0-9502
0.8702
0.8002
0.7101
0.6201













-------
               i; li A V I  M K T li  I  C    !•' 1 0 W   K X I' M R J M K N T !5
Hun:
Dry Weight:
Deflection:
S02:
Carbon:
lOO.H* mg.
-5-53 mg.
2000 ppm
EXV-3B
NO:   0 ppm

HgO:  6%
t:    200°F
                                                Ft:
Correction:
Date:
1500 cc/min.
77. OU
0.5031
May 1*, 1971
Time
minutes
1
2
3
li
5
C
7
H
9
.10
\?
Ill
16
18
20
25
30
35
140
U5
50
55
60
65
70
75
80
B5
no
."10
;>?o
:• -;o
;-'iO
Load
:r:G. llgSO^/g. C
6.09
7-39
8.29
9.. 19
10.19
:n .08
K',08
.13.08
Hi. OH
J5.08
17. ?8
19. W
. 21.77
2^.07
26Ji6
32.75
39. 7U
^7-23
55-12
63-i+l
71.50
79.79
88.18
96.56
105.25
313.7li
122.1.3
.130. IIP
.138.51
.1)16.60
15)1.38
169.66.
lH)i . Di
.197.82
2.10.80
223.19
235.17
2)16.^5
257. OH
^if.7.0?,
27''». 21
?;>i.yo
292 . w
>3VY
.1 . (",038
1 . 55?8
1 . 5029
l.kk&O
1.3980
1.31 (31
1.2283
l.l]8)i.
1.0036
0.8838
0.7639





                                    406

-------
C, K A V I M K T R  I  C   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
H47-G
103.3 nig.
-5.26 mg.
2000 ppm
EXB-2
NO:
02:
HgO:
t:

                       0 ppm
                       200°
Correction:
Date:
1500 cc/min.
76.11
0.14970
May 6, 1970
Time
minutes
1
2
3
It
5
6
7
8
9
10
12
l!|
16
18
20
25
30
35
40
't5
50
55
60
65
70
75
80
85
90
95
100
3 10
320
.130
:iiio
150
.160
170
J8o
i_yo.
poo
210
?20
230
PUO
Load
ing. H2S01|/g. C
li.26
5.52
6.29
6.97
7-65
8.23
8.81
9.ii9
10.07
10.711
.12.00
13.36
l)i. 81
16.16
17 -.62
.21.20
2)4.97
28.9't
32.81
37.07
l»l.62
k6.U6
51.78
57-10
62.62
68.23
7h. ll)
.80.33
86.53
9?. 82
99.?1
:n?.?7
:ip:..f«:
!;•!«. 99
35J -86
l6li.)|)i
r/A.)|)i
•i ' ' '. ) -pi
!<:•>, •) )
1 ' )<).>'/>
PI 1.1 9
;>:•;'. 13
>",:?. 68
^ij.ox
253.. 19
r6P.it 9
Mean Load
mg. HgSOj^/g. C
2 n
k
6
8
10
... 12
Ik
16
18
20
25
30
35
1)0
)i5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
l!|0
.150
160
.170
180
190
P.OO
??Q
P)|0
:-'6o






Rate
mg. li^SO^/s. C/:ain.
k. 355^
2.14.003
0.77^3
0.6775
0.6581
0.658.1
0.6630
0.6727
0.6872
0.7065
0.7598
0.8227
0.8808
0.9388
0.9872
i.0308
1.07^3
1.1130
1.1518.
1.1905
1.2292
1. 2W5
1.2679
1.2873
1.2969
1 . 3066
1.3163
1.3163
l . 3066
1.2969
1.2776
1.2582
1.2389
1.2098
1.1808
.1 .1518
.1.0889
] .()!(>•{
Q.<)WV,






                    407

-------
GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon :
154-G
117.04 mg.
-5-53 mg.
2000 ppm
EXA-1
NO:
02:
HjO:
t:

                       0 ppm
                       200 °F
!t!
                                            Correction:
                                            Date:
1500 cc/min.
71.24
0.4652
May 26,  1971
Time
minutes
1
2
3
)|
5
6
•(
0
9
JO
.1?
14
16
18
20
25
30
35
40
45
50
60
70
80
90
:ioo
.110
.IPO
J'J,0
I'lO
11)0
160
.170
180
190
?00
?10
220
?30
?l|0
250
tf>0
270
r.".o
?' )0
"<00 j
Load
r,ie. H2S01(/g. C
0..17
0.34
0.60
0.77
0.94
.1 . .1 1
1.37
.1 . 5'i
1.79
1.97
2.31
2.73
3-08
3.42
3-67
4.53
5-30
6.07
6.75
7-43
8.03
9.31
10.li2
11.53
12.65
13.67
.Hi. 70
_Lk- 5>
1 6 . V
l/.oy
jy.f")
18.37
39.22
20. ?'j
21 . 36
22.73
2)|..l8
25-72
27-17
28.96
30. y>
3?.3U'
3'i.l»
3«i. 'V.
:;7.M.'i
;'».fl,"
Mean Load
mg. H^SOj/g. C
2
It
6
8
10
-, 12
:4
16
18
20
22
24
26
28
30
3?
34
36
38
40


























Rate
mg. HgSOjj/g. C/min.
0.2153
0.1692
0.1393
0.1?56
0.1128
0..1008
0.0897
0.0705
0.0880
0.109)1
0.1282
0.1427
0.1521
0.1623
0.1692
0.1777
. .0.1837
0.1897
0.1931
0.1965


















^







                     408

-------
  0 R A V 1 M !•; T K I C   F 1, 0 W   EXPERIMENTS
Run:         J5'j-G
Dry Weight:  108.52 mg.
Dofleetlon:  -5-85 mg-
             2000 ppm
D02:
Carbon:
                                 NO:   0 pprj
                                 02=   3-5V
200°?
                                                Ft:
                                                Correction:
                                                Date:
1500 cc/rain.
76.99
0.5028
May 27, 1971
EXB-3
Time
minutes
1
2
3
It
5
6
7
8
9
10
.12
lit
16
18
20
25
30
35
itO .
1*5
50
55
60
65
70
75
80
85
90
95
100
110
.120
J30
DK>
J',0
1 60
JYO
JfiO
1 <>0
,'•00
;MO
;-20
:?_;0
piio
250
260
270
p8o
?90
300
Load
ing. H2SO),/g. C
3.87
14.88
5.62
6.36
7.10
7-83
8.57
9-31
10.014
10.78
12.35
13-91
15.57
17-23
18.89
23. Ill
28.20
33-27
38.89
U5.06
51-33
57.96
61*.. in
70.77
77.22
83.76
91.23
98.51
105-79
113. .16
120.53
135-09
lfi9-37
: 6:^.38
177.29
iyi.9!>
;;o6.oii
;?io.f,«
;>•<•. 58
:'Mi.66
;">:.;. oo
r>< />.('.«
PYY . oo
;>«.•,. <>:,
P<'6.17
•j,o'i . or1
^i3.f.i
:;;o.05
;::'3.05
.Tj'i-9'S
3)12.06
Mean Load.
mg. H2SOi+/g. C
2
1*
6
8
10
12
lit
16
-- 18
20
25
30
35
1*0
»I5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
ll)0
150
160
170
180
.190
200
220
2liO
?60
;-ao
••jOQ
320
3liO








Rate
mg. H2SO^/g. C/min.
3-8703
1.9812
0.7925
0.7l)-6^
0.76148
0.7833
0.8109
0.8386
0.8662
0.8938
0.9583
.1.0229
1.0781
1.12142
. 1.1703
1.2072
1. 2l4l40
1.2809
1.3085
1.3362
1.3638
1 . 3822
1.1(007
1.14191
1.^375
DA67
1.14652
1.1471414
l.VfWk
1.1)652
1.U560
1.^375
1 . li099
J . 391)1
J • 3638
l .330?
l.?
O.'W^l
O.R017
0.6'OJ








                       409

-------
               i; H A  V  I  M K T H 1  C   !•' I. <> W   K  X  1' K  K I  M !•! N T !'.
Hun:         3 >(>-(";
Dry Weigh' :  103.60 ing.
Deflection:  -5-90 i::g.
             2000 ppra
             EXC-1
NO:   0 pp:n
02:   3-5"
H20:
S02:
Carbon:
Time
minutes
3
2
3
)i
5
6
y
8
9
10
12
Hi
16
18
?0
25
30
35
1*0
145
50
55
60
65
70
75
80
t'j
90
0';
.1.CX)
no
.12(1
1 -if)
l'in
!'.)<)
ViO
jyo
IMO
1Q( >
20d
2.10
220
2<0
2UO
2'/>
P-.0
270
,'^••0
L>'»U
•iOO
Load
me- H2::o)(/g. c
9.27
10.1(2
31.29
12.16
32.93
33.80
Di.67
15.1('i
16.33
37.30
18. H2
20.66
22.39
2U.33
25-97
30.60
35-52
1+0. 61*
l*6.ll*
51. 7!*
57-53
63.51
69.50
75.68
81.76
88.03
oH.2l
100. ^9
106 . r>G
132. 8'i
3.:i-).i3
13.1. 1 H
1 1(2. <.>5
iVl.'l'i
,lf.',.r,l|
jyi'..'1'.j
.!(''.. '17
]<>Y.10
2i • .1,1')
23.i.,.>'i
22-\. Ij
2 -U.' . ;i J,
2lfO.S-l
2lj';.,,S
2'ii', . 3..S
• 1, , . '")
27>\,'7
jy--."-;
^•i.-':fi
^•••'.'is
;M'i.]y
                                  t:
      200 CF
                                                               Ft:
                                                               % HgSOj,.:
                                                               Correction:
                                                               Date:
1500 ce/min.
75-15
0.1*908
May 28, 1971
Mean Load
mg. HgSO^/g. C
6
8
10
12
Hi
16
38
-, 2.0
25
30
35
l|0
1)5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
l'*0
350
160
iyo
.180
190
?_oo
220
ii'lO
2/,0
280
.












Rate
mg. H2SO^/g. C/min.
7.1i*29
1+.1988
1.1390
0.8687
0.8301
0.8398
0.8591
0.878)f
0.9266
0.97^9
.1.0232
1 . 0?lU
1.100)i
1.1293
1.1583
1.1873
1.1969
1.2162
1.2259
1.2355
1-2355
1.2355
1.2355
1-2355
1.2259
1.2162
1.3-969
1.1680
l.lif«6
1..U97
1.0907
. 1.0610
1.02 =52
().
-------
GRAVIMETRIC  FLOW  EXPERIMENTS
Run:
Dry Weight:
Deflection:
SO :
Carbon :
159-G
102.26 mg.
-5-93 mg.
2000 ppm
EXA-2
NO:
V
HO:
tf

0 ppm
3-5*
%
200° F

                                            '.V
             1500 cc/mln.
             79- 44
Correction:   0.5188
Date:         June 7, 1971
Time
minutes
1
2
3
>t
5
6
7
. 8
9
10
12
14
16
18
20
25
30
35
ho
45
50
60
70
Ro
VO
100
11,0
120
1.30
I'lO
150
160
170
180
190
200
2.10
' ??0
230
2'c.)
no
260
','/0
?.",o
;>• m
300
Load
ng. H2SOl,/g. C
2.64
3-52
3.91
4.20
li.'jO
k.(f)
II.B-J
5.0^
5.28
5.38
5.67
5./r
6.26
6.55
6.75
7-53
• 8.31
9-00
9.68
10.37
11.05
12 . 52
13.89
.15-45
Jfi.'tf
I,",J|H
19-95
21.51
P3.0H
24.64
26.31
i'7-07
29-73
31 • 39
33.15
31' • 91
36.77
3>"-63
ii0.5»
ii;;.54
hh.'j-*
46//4
4't.H'i
51..24
'>V'>
56.13
Mean Load
ing. HaSOlj./g. C
4
6
8
. 10
••' ie
1)1
16
18
20
25
30
35
40
45
50
55






























Rate
nig. HgSO^/g. C/min.
0.3071
0.1604
0.1408
0.1418
0.1438
0.1457
0.1486
0.1516
0.1555
0.1633
0.1741
0.1868
0.2005
0.2151
0.2318.
0.2494












•

















                     411

-------
GRAVIMETRIC  FLOW  EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
165-G
106.92 mg.
-5-97 mg.
2000 ppm
EXA-3
NO:
02:
HgO:
t:

0 ppm
3-5$
656
200° F

t
                                                       1500 cc/min.
                                              2h:     77-85
                                           Correction:  0.5084
                                           Date:        June 16,  1971
Time
r.inutes
1
2
3
4
5
6
7
8
9
10
12
14
16
10
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
140
150
1 60
170
180
190
POO
?10
2PO
'30
shn
'50
•('/>
'(<>
;'r>
> .-)8
^'i?.70
',"j\ . »'.
;'u).4'(
;'i»i'.".o
'.''(<'••'/>
:''-'J.v'"
P "l.l.-',
P >{. I'l
•^05.40
•jo i.'iM
:. 03
•]..Y'l
Mean Load
mg. HpSOjj/g. C
	 	 • • ' — ' ' "
2
4
6
• 8
-'10
12
Ik
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
3.40
150
160
170
180
190
POO
220
2l)0
260
?;*o
300
3?o







Rate
ing. HpSOk/g. C/rain.
4.2088
2.5907
1.6835
1.1785
0.9727
0.8605
0.7669
0-7202
0.7108
0.7295
. 0.7856
0.8230
0.8698
0.9166
0.9540
J. . 0007
1.0382
1.0156
1 • 1130
1.1504
1.1785
1.2065
1.2252
1.2439
1-2533
1.2626
.1.2813
1.283.3
• 1.2720
1.2626
1.2439
1.2252
1.1972
1.1691
1.1504
1.1130
1.0382
0.95)10
0.8605
0.766)
0.6640
0 . 563 f>







                    412

-------
GRAVIMETRIC  PLOW  EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
166-0
101.36 mg.
-6.09 mg.
2000 ppm
EXA-4
NO:
02:
HgO:
t:

0 ppm
3-5$
6$
200° F

Ft:
Correction:
Date:
                                                         1500  co/tnin.
                                                         77.20
                                                         0.5042
                                                         June  21, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
10
12
It
16
18
20
25
30
35
40
45
50
60
70
80
90
100
110
120
130
I'lO
.100
.1.60
J.YO
.1 HO
1 'X>.
;?oo
21.0
;vo
;>30
P'lO
250
260
270
2MO
2-)0
'•(00
Load
ing. H2SO^/g, C
4.o4
5.82
7.20
8.29
9.27
10.26
11.25
12.33
.1,3.32
lit. 31
16.18
18.15
19.93
21.80
23.78
28.12
• 32.66
37.19
iH. 83
46.47
51.30
61.76
73-01
84.55
96.98
110.00
12P.93
135.06
l4Y.'lO
1 V.i. 83
172.36 . . . .
LS'l . 19
.1 >J'j . Y'l
;K>6.3v
P,l/).'j'3 . ..
226. >'!
23S.Y9
P'i4.0Y
2V-;.B'j
Pfr'.Oli-
069. »3
2YY.'t3
2811.63
291.5'!
2->H.L5
30'i . 66 . ... ...
Mean Load
mg. H2SOij/g. c
2
.4
6
8
' 10
12
14
16
18
20
25
30
35
40
45
50
55
60
65
70
75
80
85
90
95
100
1.10
120
130
140
150
160
170
180
190
POO
220
240
260
280
300





Rate
mg. HgSO^/g. C/min.
4.0450
2.4862
1.6180
1.1346
1.0359
0.9767
0.9471
0.9373
0.9274
0.9175
0.9077
0.9126
0'.9175
0.9422
0.9570
1.0014
1.0359
1.0754
1.1099
1.1444
1.1691
1.1938
1.2135
1.2332
1.2480
1.2579
1.2727
1.2727
1.262H
1.2579
1.2382
J .2184
1.1938
I.l6)i2
i.J3'i6
1.0951
1 .0162
0.0274
0.828Y
0.7202
0.6215





                     413

-------
GRAVIMETRIC  FLOW  EXPERIMENTS
Run:
Dry Weight:
Deflection:
S02:
Carbon:
167-G
107-14 mg.
-5-99 mg.
2000 ppm
EXA-5
NO:
02:
H20:
t:

0 ppm
3-5$
6$
200°F

 t
Correction :
Date:
                                                       1500 cc/min.
                                                       77-51
                                                       0 . 5062
                                                       June 23,  1971
Time
ninuteo
1
2
3
4
5
6
7
8
9
10
12
14
16
18
20
25
30
35
40
45
50
60
70
80
90
.100
no
IP'O
1.30
UlO
1^0
160
170
180
1^)0
?00
210
?J.'0
•30
J'|0
•"jO
'l:i)
'(()
': '•< )
'•)•}
•sou
Load
inc. HgSOjj/g. C
3-17
4.67
5-69
6.53
7-37
8.12
8.87
9.52
10.17
10.83
12.13
13.44
14.75
16.15
17-55
21.09
24.64 .
28.19
31-83
35-56
39.39
47.23
W-44
64.60
74.30
84.66
95-30
106. 4 o
117.51
128.62
139.54
I.b0.64
161.56
172.58
J83.22
193. 2 L
202.91
212. 'j 3
22L.95
231.10
2S'.'.';/1
PW.iM
P'jY.'jl
f'(,fi.".j
L'lV.OY
;>Y;i.:(...
Mean Load
ing. HgSOjj/g. C
2
4
(>
8
' 10
12
14
16
18
20
25
30
35
ho
45
50
55
60
65
70
75
80
85
90
95
100
110
120
130
i4o
150
160
170
180
190
200
220
240
260
2MO






Rate
mg. l^SO^/g. C/min.
2.7067
1.6054
0.9_520
0.7467
0 . 7000
0.6814
0.6720
0.6814
0.6860
0.6907
• 0.709^-
0.7280
0.7560
0.7840
0.8167
0.8494
0.8867
6.9240
0.9614
0.9894
1.0080
1.0360
1.0500
l.o64o
1.0780
l . 0420
l . 1060
1 . .1 107
1.1107
.1.3014
1 . 0920
1.0780
1.0594
1.0407
1 . 0174
0.9894
0.9334
0.8yi7
0.7840
0.70^4






                     414

-------
GRAVIMETRIC
FLOW
                                   EXPERIMENTS
Run:
Dry Weight:
Deflection :
S02:
Carbon:
if, 9- a
100.50 ing.
-5.91 n«-
2uOO ppm
]•:>:••;- 4
NO:
02:
H20:
t:

0 ppm
3f~ ^
• )"!'
6%
200° F

                     Ft:
                     Correction:
                     Date:
                                                          1500 cc/inin.
                                                          78.24
                                                          0.51105
                                                          June 25, 1971
Time
minutes
1
2
3
l)
5
6
7
8
9
10
12
lit
16
18
20
25
30
35
ho
45
50
60
70
80
90
100
110
120
I'-JO
.11)0
150
IhO
.170
IMG
J'lO
2UO
2.1 n
220
2-iO
2-'.0
2''0
;>r,o
270
,''',(}
','.'l<>
':< )0
Load
m.";. H230i|/(;. C
1+.73
6.17
7.06
ti.or,
8.96
9.95
10.95
11. 9'J-
12.9U
13-93
16.02
18.31
20.50
22.89
25.17
30.95
37. lH
Mt.68
52. Mi
60.80
69.65
88.36
107.96
128.26
11*9.25
169.75
189.75
20H.96
226.97
2l)3.(.rt
2!>Q.oO
275-02
|_ 290.05
30.5 . 08
l.Tt.'H
•J,20.''7
j, j,<,. ','.:>.
Vin. 17
V..'.. :2
V l-'l .'..')
W.2'i
•;7< I . ' in
••.-.7.1"
-.••••I.IM
)|E 1 ] t\>> t
h>>{.'/t.
Moan Load
rng. HaSOl^/R. C
1)
6
8
10
-' 12
14
3.6
1.8
20
25
30
35
Uo
45
50
55
60
65
.70 .
75
80
85
90
95
100
110
120
130
1.40
150
160
170
180
190
200
2.?0
2'lO
2f,0
2MO
HOO
•;HO
••;'iO
•li .0
VH>
lino

Rate
mg. HjjSO^/g. C/min.
3-l«4l
1. 2'I38
0.9254
0.9552
0.9751
1.0149
1.0348
1.0647
1.0945
1.1741
1.2637
1.3433
1.4229
1.4975
1.5672
1.6418
1.7015
1.7612
1.8109
1.8607
1.8905
1.9204
1.9602
1.9900
2.0100
2.0498
2.0697
2 . 0796
2.0796
2.0697
2.059V
2 . 0398
2.0000
1.9'".C2
l.Ol.Oli
1.7"' 0
l.
-------
G R A V I M K T H I C   ]•' L 0 W   K X P K H I M E NTS
I'uri:
Dr.y WeM'L:
D< •riwt.jon:
C02:
Carbon:
1.7"-'!
.Kv'.'.'i nit'.
-5. 'i.l me,.
2000 ppm
EXB-5
                   NO:
                   HgO:
C) ppm
3.5$
6*
200° F
]?t:          3-500 I'
$ HgSOj,:     78.4?
Correction:  0.532)4
Date:        June 28, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
10
32
3.1)
36
3.8
20
25
30
35
Uo
>45
50
60
70
80
90
100
110
120
HO
1'jO
ISO
'li.U
170
i.'-;o
3 ' '0
2oo
23.0
2.-i '
2 -;(.'
.-.'llO
2M>
i.'i i)
270
2.''d
2' 40
J,t «.)
J, It)
j- );^
•> -ll '
Load
mr.. T!?SOb/«. C
U.19
6.33
7.79
8.87
9-9'*
11.01
32.08
3.3.06
13-93
1)4.71
16.56
3.8.61
20.65
22 .<>0
25-23
31.18
37.61
14)4.72
52.51
60.80
69.66
88.56
108.73
329.87
150.lt|
170.01
188.91
206.55
223-79
2'i0.55
2y>.M
27.1.. 0)+
2M . 3 0
2'i',.8i,i
307. f»
-11'".. 00
•:2».5i
', ;.-f.O^
•;'ii,.(.S
-;•-']. is
','•1 .in,
-;.,".. |.-i
'.Y'«.< !
'.-'. 1 .»'li
-•,--;y.2,;>.
•;• i -i . .12
••.•i.".. 87
)K''I .o-j
llU'^.UO
Mean Load
mg. H2SO^/g. C
2
If
•6
8
10
12
14
16
18
20
25
30
35
1)0
'45
50
55
60
65
70
75
80
85
90
95
100
1J.O
320
130
lUO
.1.50
160
370
180
wo
200
220
2*10
A ,0
2H<>
',00
^20
.)l|0
-:f'.o
--i»o
InOO



Rate
mg. HgSO^/g. C/min.
^. 38)43
2.7280
1.5680
1.^322
1.0035
0.9353
•0.9256
0.9^99
0.98^0
1.0279
I.l₯t8
1.2U22
1.3396
3..U322
1.5101
1.5881
1.6660
1.73^2
1.7927
1.8)463
1.8950
1.9339
1.9729
1-9973
2.0216
2.0)460
2.0703
2.0752
2.0703
2.0557
2.02.16
.V.9B75
1.9)186
l . 90uf>
3.H706
1.8.1YO
3..7050
l-'/C-'V-i
i.'i m.
3 .271--!
1..I2())J
D.')7'H
o.^v/o
0.7210
o.r.oaq
0.52bl



                     416

-------
                r, K A V I  M K T li T C   V T, 0 W   V X I' K R T M K N T I',
Run:
Dry Weight:
Deflection:
S02:
Carton:
171-C!
101.80 nig.
-6.22 mg.
2000 ppm
EXA-4
Time
minutes
1
2
3
14
5
6
•I
8
9
.10
X?
3.4
16
18
20
25
30
35
1+0
U5
50
60
70
80
90
100
330
120
1 '.()
1.4 0
I'/'
K.d
:iY''>
.U'f'
]nO
21 >'')
2JO
22"
2-:o
24 o
2',...
2.'0
270
2.' 0
2' -C>
•inn
Load
mg. HgSO^/g. C
5-50
7-56
9.014
30.32
11.. 20
12. 2H
13-26
lH.35
1^-93
l'j.82
37-°'.)
3.8.76
20.04
21.U1
22.99
26.82
31.04
• 35-66
1*0.37
U5.28
50.29
60.81
71.51
82.91
9'i-79
.106.88
31 9- 35
131.93
l.'i'i.Ol
.V/-.80
l(>7.r;<'i
17H . * .rt
380.30
.v>',).:i2
2i'.'i.Wi
23.8. liy
227.70
236.7!)
24S.68
2[.;'i . .«
2i..-!.'-!7
270.02
2V.J.2M
2J-.4.7.7
?•>').{•'('
;?»...*>•;
J2'
U2C
t:
H20:
0 ppm
3.536
e*
200° F
                          *t:
             1500 cc/niJn.
             77.04
Correction:  0.5031
Date:        June 29, 1971
Mean Ixsad
mg. HgSO^/g. C
2
It
6
8
10
"' 32
lit
16
18
20
25
30
35
ItO
it5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
140
150
3/.0
170
18'0
190
200
220
240
260
280
300





Rate
mg. HgSO^/g. C/min.
6.5815
3-6337
2.4558
1.5226
1.2083
0.9921
0.874.3
0.7«59
0.7466
0.7367
0.7957
0.8^46
0.9037
0.9627
0.9921
1.0314
1.0609
1.0904
1.1198
1.1395
1.1591
1.1788
1.3886
1.2083
.1.23.81
3.. 2279
1.2377
1.2475
.1.2 ',77
.1.21 H.I
J.lHHi,
1 ..l'/)l
3 . 1297
3 .1002
1.0609
.1.02.16
0.9528
0.8743
0.7859
0.6876
0 . 5094





                                      417

-------
r; R A v :i M !•; 'i1 K i c
                          LOW   K X ]' K K 1 M E N T !i
Him:
Pry Welch t:
Deflection :
S02:
Carbon:
172- G
100. ll* m;'..
-6.13 mg.
2000 ppm
EXC-2
NO:
02:
H20
t:

                          0 ppm
                          200° F
Ft:          1500 cc'/rain.
% H2SOi+:     76.89
Correction:  0.5021
Date:        July 8, 1971
Time
minutes
\
2
>>
1(
5
(',
7.
B
9
1.0
.12
111
16
18
20
25
30
35
1(0
'45
50
60
70
HO
90
100
110
.120
.1 «)
ll|()
ISO
-|.'.Q
17U
I.'"-)
I'/O
;_'-.o
..' 10
.'.w
?.'-.<•>
•^«
.?'.o
' 'i "
,-yo
':'• '-ll
.' "'
',()!)
Load
me.. H2SOj,/c;. C
i JlO
5 • 19
(>. -iO
7.S')
H . vy
•).2'i
K). 19
1i).')M
11. HM
' 12. (',8
I'l-.'iH
16 . 1.7
17-97
19.87 .
21.77
26.86
32.15
37.85
1*3.714
50.33
57-02
71 . 10
«fj.f,8
.10^.26
.ll'i.'M
l',f,.K.I.
J5',.7'
170. ','•
j. '-;,,. N'I
2ul .22
<-'!'.. 1.0
iNo. •;•:
2Mi.)|,,
2'>-.2i4
271.52
2 U..-M
2- "1. 7s.'
-iill .'•.-.
•i.'.ir.
^ . i -.
•MI .«.';
•''- '.'>.?
•.' '.11
•'.....' u
.1 •; . ' .' i
V(".i .'>
                     418
Moan Load
me- l^SO^/g. C
2
l|
6
.•- 8
10
12
111
ir,
18
20
25
30
35
ko
1+5
50
55
60
65
70
75
80
85
90
.95
.100
.1JO
.120
1 J,0
1'40
150
160
170
.1.80
190
200
220
2UO
2.'0
280
WO
#0
•s'.o
Vfl


Rate
mg. HgSOjj./g. C/min.
2.9^59
]..877'i
1.2l|«3
0.9087
0.8238
0.0.1H9
O.H'MH
0.87.-S8
0.9*7
0.9J87
1.0136
1.0/85
l.lUSlf
1.2033
1.2582
1.3132
1.3581 •
1.1*030
1.14-1*30
1.1*779
1.5179
1.5W
1.5728
1.5978
.1 .6177
:i .6 <77
.1 .u;a
•l.''77Y
)..^Hr!d
l.C>777
l.f.f.77
I.c,'i77
1.6227
1.5978
1.5678
1.5279
l.'*530
1. 368.1.
1.2682
J . 1.68'i
J .oi>8s
0.
-------
GRAVIMETRIC   FLOW   EXPERIMENTS
Run:
Dry Weight:
Deflection :
S02:
Carbon:
175-G
102. 56 ing.
-6.16 ing.
2000 ppra
EXC-3
NO:
02:
H20:
t:

0 ppm
3.5%
6.0$
200° F

t
                                                        1500 cc/min.
                                                        73-58
                                            Correction:  0.1+980
                                            Date:        July 16, 1971
Time
inj nutos
1
2
3
k
5
6
7
8-
9
10
12
lit
16
18
20
25
30
35
1+0
U5
50
60
70
80
90
100
110
120
130
l!|0
150
160
170
180
300
200
230
<«(>
2 '•',()
2'iO
2'.<0
?V>0
270
2.<<>
2')0
3(10
Load
ing. HgSOli/K. C
6.3^
8.29
9-5<>
10.l|\
11.31 -
12.09
12.77
13.W
1H.1.1+
1.1+.72
16.19
17.55
19.01
20. 1*8
22.01+
26.23
30.91
. 36.08
lU.Mt '
1*7.19
53-33
66.50
80. 5'+
95- H6
1.10.18 .
125-39
lit 1.38
157.37
172.87
.188.09
201.93
21.lt. 90
228 . 16
21(1.22
253- Jil
265. Ill
276. <0
.2H7.(i'i
2', ,'7. 00
'.U) . IK'I
.', I'l .'i)|
32 x.('.r;
^1.71.
•i -i'-).ii.i
',iir,.;,;!
Hr< '<.')'(
Mean Load
mg. HgSOl^/g. C
2
1+
6
8
10
-, :i2
ii*
16
18
20
25
30
35
1+0
't5
50
55
60
65
70
75
80
85
90
95
1.00
110
120
130
1^0
150
160
170
180
190
200
220
21+0
260
280
300
320
i'K)



Rate
mg. HgSOij/g. C/min.
8.239],
5 • 1677
3.120.1
1.7'i53-
0.8970
0.7110
0.6533
0.6728
0.7215
0.7605
0.8678
0.9555
1.0238
1.1018
1.1603
1.21.88
1.2676
1.3066
1-3358
1.37W
i.i+oin
1A333
1.1(528
lA?23
I.li91.8
1.5113
.1.5308
1.5503
1.5601
1.5601
1-5503
1.5308
1.5113
1.U821
l.Ul+31
l.l+oUi
1 . 3066
1.2188
1.1.1|08
1.0628
0.0653
0.8678
0.760',",



                     419

-------
                        APPENDIX A-15-2
           SURFACE AREA AND PORE VOLUME DISTRIBUTION
                  OF SOLVENT EXTRACTED CARBON
  Surface area and pore volume distribution measurements were
  made by means of nitrogen isotherms on the Englehard Isorpta,
  Englehard Industries, Inc., Newark, New Jersey.  The surface
  area was calculated from the BET equation12* and the pore
  volume distribution with a computer program we have using the
  Roberts13 method of pore determination.  In the tables given
  in this section, REL P is relative pressure and VOLUME is
  volume adsorbed of nitrogen in cc./g. C.  Other designations
  are S = surface area in m2/g. C; C = the BET constant, and
  R = the correlation coefficient.  PORE RADIUS is the range
  of pore size in A; VOL is the volume in cc./g. C in that
  range; and CUMV is the cumulative volume to that point.
     *References are listed in Bibliography,  Section 8,  in
Volume I.
                             420

-------
        SAMPLE:  EXA-1
    RFL  P
v/OLUME
U. 1423
o. i 7a2
0.2141
0. 3219
0.4296
0.5374
0.6452
0. 7529
O.t,607
0.9685
S 193.
C -34
R 0.9980
0.09.13
0.0990
0.1015
0.1078
0.1135
0. 1182
0.1226
0.1260
0.1318
0.1389
7
.257

PORE RADIUS
     VOL
CUMy/
1000.
500.
400.
300.
200.
150.
100.
90.
dO.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
U.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0012
0.0006
O.OOC9
0.0016
0.00 I1* "
0.0027
0.0009
0.0011
O.OC13
0.0017
0.0021
0.0015
0.0018
0.0022
0.0029
0.0043
0.0063
0.0041
0.0055
0.0070
0.0076
A. 0.0114
0.0012
0.0018
0.0026
0.0042
U.OObY
O.OOt'4
0.0093
0.0103
0.0116
0.0133
0 . 0 lt> 7
0.0172
0.0191
0.0213
0.0242
0.0285
0.0353
0.0394
0.0449
0.0519
0.05vl>
0.0700
                  421

-------
          SAMPLE:  EXA-2
REL P
VOLUME













PORE
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
0.1488
0.1865
0.2243
0.3375
0.4508
0.5641
0.6773
0.7906
0.9039
0.9869
S 167.7
C -28.
R 0.9991
RADIUS
500.
400.
	 300. 	
200.
150.
	 100. - -
90.
80.
70.
60.
50.
45. 	
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0856-—
0.0878
0.0900
0.0966 	
0.1028
0.1003
0.1133 	
0.1180
0.1234
0.1287 .-

132

VOL
0.0009
0.0004
	 0.0007 	 	
0.0013
0.0012
0.0023 — 	
0.0008
0.0010
0.0012
0.0016
0.0023
--0.0015 	 	
0.0019
0.0024
... .. . 0.003i
0.0048
0.0078
0.0047
0.0059
0.0070
0.0077 	 	
0.0077













CUMV
0.0009
0.0013
0.-0020 	
0.0032
0.0045
0.0068 	 - 	
0.0076
0.0085
0.0097
0.0113
0.0136
0.0151 	
0.0170
0.0195
0.0227
0.0275
0.0353
0.0400
0.0459
0.0529
0.0606 " ' '
0.0683
                 422

-------
           SAMPLE:  EXA-3
REL P
VOLUME













PORE
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
lb.
16.
14.
12.
0.1488
0. 1865
0.2243
0*3375
0.4508
0.5641
0.6773
0.7906
0.9039
0.9869
S 	 650.9
C -20.
R 0.9983
RADIUS
500.
400.
300.
200.
150.
— 100. -
90.
80.
70.- 	
60.
50.
_._-_... 45.
40.
35.
30. 	
25.
20.
18.
16.
14.
12.
10.
0.3620
0.3684
0.3731
0.3850
0 . 3 94 8
O.'»027
0.4096
0.4161
0.4231
0.4296-- •
•
340

VOL
0.0010
0.0005
0.0008
0.0016
0.0015
	 0.0029 	 - 	
0.0010
0.0012
- 0.0016 - -
0.0021
0.0030
— 0.0021 	
0.0026
0.0034
	 0.0045 	 -
0.0066
O.Olll
-- 0.0071 	 	
0.0094
0.0120
0.0151 	
0.0210













CUMV
0.0010
0.0015
0.0023
0.0039
0.0054
0.0084-
0.0093
0.0106
0.0121 	
0.0142
0.0173
-0.0194 	
0.0220
0.0254
-0.0299
0.0365
0.0476
0.0547
0.0641
0.0761 "
-0.0912
0. 1122
                 423

-------
    REL P
             SAMPLE:   EXA- 5
VOLUME
0. 1428
0.1791
C.2153
0.3241
0.4328
0.5416
0.6504
0.7591
0.8679
0.9766
0.3382
0.3430
0.3478
0.3588
0.3683
0.3759
0.3831
0.3898
0.3975
0.4093
     S    620.8
     C     -22.416
     R  0.9985
PORE RADIUS
     VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0026
O.OG10
0.0015
0.0026
0.0023.
0.0041
0.0013
0.0015
0.0019
0.0025
0.0035
0.0024
0.0029
0.0036
0.0048
0.0069
o.oion
0.0066
0.0092
0.0117
0.0133 -
0.0201
0.0026
0.0037
0.0052
0.0079
0.0102
0.0143
0.0155
0.0171
0.0190
0.0215
0.0250
0.0274
0.030H
0.0339
0.0387
0.0456
0.0564
0.0630
0.0722
0.0840
0.09'M
0. 1174
                    424

-------
          SAMPLE:  EXB-3
    REL P
VOLUME
0.1426
0. 1788
0.2151
0.3237
0.4323
0.5409
0.6495
0.7581
0.8667
0.9753
S 667.
C -22
R 0.9986
0.3636
0.3690
0.3734
0.3855
0.3956
0.4039
0.4115
0.4184
0.4257
0.4350
5
.456

PORE RADIUS
     VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0015
0.0007
0.0010
0.0019
0.0018
0.0034-
0.0011
0.0014
0.0018
0.0024
0.0034
0.0023
0.0029
0.0038
0.0051
0.0074
0.0119
0.0073
0.0097
0.0125
0.0156
0.0187 -
0.0015
0.0022
0.0032
0.0051
0.0069
0.0104
0.0115
0.0129
0.0146
0.0 1 70
0.0204
0.0227
0.0256
0.0294
0.0345
0.0419
0.0538
0.0611
0.0708
0.0833
0.0990
0.1176
               425

-------
           SAMPLE:  EXB-4
    REL P
    0.9741
VOLUME
0.1425
0.1786
0.21^8
0.3232
0.4317
0.5402
0.6487
0.7571
0.8656
0.3720
0.3772
0.3816
0.3931
0.4023
0.4100
0.4167
0.4237
0.4309
0.4407
     S    680.1
     C     -22.182
     R  0.9986
PORE RADIUS
     VCL
CUMV
1000.
500.
400.
30U.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40. .
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0021
0.0008
0.0013
0.0022"
0.0020 '
O.OC35
O.OOll'
0.0014
0.0013
0.0024
0.0034
0.0023
0.0030
0.0039
0.00.49
0.0063
0.0106
0.0068
0.0089
0.0115
0.0148
--•0.0189
0.0021
0.0030
0.0042
0.0064
0.0084
0.0119
0.0130
0.0144
0.0162
0 . 0 1 b 5
0.0219
0.0242
0.0272
0.0310
0.0360
0.0423
0.0529
0.0597
0.06U6
0.0800
0.0948
0.1137
                   426

-------
       SAMPLE:   EXB-5
REL P
VOLUME
.. -












PORE
1000.
500.
400,
300.
200,
	 150*
100.
90.
80.
-- - - \f *^ w
70.
60.
50»
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
0.1484 ...
0.1860
0.2237
0.3366
0.4496
0.5626
0.6755 	
0.7885
0.9015
0.9994 ....
S 	 -73K4
C -19.
R 0.9983
RADIUS
500.
400.
	 300. 	
200.
150.
	 100* 	
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
o.4ioa 	
0.4169
0.4213
0.4334_ __,_.
0.4439
0.4530
0.4 60! 	 ,_.
0.4679
0.4756
0.4842

859

VOL
0.0011
0.0005
	 0.0009_.^...
0.0017
0.0017
... 	 0.0032... ..
0.0011
0.0013
0.0017 .
0.0023
0.0034
u 	 O.OQ24
0.0030
0.0038
0.0051 . ..
0.00/3
0.0128
0.0080 .
0.0102
0.0125
0.0148
0.0188













CUMV
0.0011
0.0017
	 	 fl.0026 	
0.0043
0.0059
._ 	 0.0091 	 	
0.0102
0.0115
0.01 H
0.0156
0.0190
o.opn
0.0243
0.0282
_ 	 0.0332
0.0405
0.0533
_ . 0.0613
0.0714
0.0839
0.0988
0.1175
               427

-------
           SAMPLE:  EXC-1
    REL  P
VOLUME
0. 1426
0. 1788
0.2151
0.3237
0.4323
0.5409
0.6495
0.7581
0.8667
0.9753
S 628.
C -22
R 0.9985
0.3442
0.3489
0.3531
0.3634
0.3722
0.3805
0.3873
0.3937
0.4007
0.4132
0
.024

PORE RADIUS
     VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0040
0.0014
0.0020
0.0031
0.0025
0.0041 •
0.0012
0.0015
0.0018.
0.0023
0.0032
0.0021
0.0027
0.0034
0.0045
0.0065
0.0115
0.0073
0.0086
0.0104
0.0127
0.0174 '
0.0040
0.0054
0.0074
0.0105
0.0130
0.0171
0.0 l»3
0.0197
0.021r>
0.0238
0.0270
0.0291
0.0318
0.0353
0.0398
0.0463
0.0578
0.0651
0.0737
0.0841
0.0963
O.U41
                 428

-------
              SAMPLE:  EXC-2
      REL  P
        VOLUME
       R
   736.8
    -20
0.9982
 PORE  RADIUS
 1000.
 500.
 400.
 300.
 200.
 150.
.100.
  90.
  80.
  70.
  60.
  50.
  45.
  40.
  35.
  30.
  25.
  20.
  18.
  16.
  14.
  12.
 500.
 400.
 300.
 200*.
 150.
 100.
 -90.
 80.
 70.
	60 »
 50.
 45.
- 40.
 35.
 30.
 25.
 20.
 18.
 16.
 14.
 12.
 10.
0.4102
0.4172
0.4232
0.4348
0.4459 	 ._
0.4553
0.4624
0.4688 	
0.4768
0.4838
t
• 304 ..
VOL
	 0.0003 	
0.0004
0.0007
0.0016-
0.0017 '
0.0035
0.0012-
_ ,. — ._— - -^0 ^ ^f %^*«r ^ff^-f-m^,
0.0015
0.0019
0.0024
0.0034
0.0021
	 0*0026—
0.0033
0.0044
. .-0.0068.-.-
0.0132
0.0086
0.0109 ..
0.0125
0.0133
- 0.0262 .-











CUMV
	 „.„_.._ 0.0003
0.0007
0.0014
0.0030
0.0047
0.0082
0.0094
0.0109
0.0127
0.0151
0.0185
0.0206
— 	 0.0232
0.0266
0.0310
	 0.0378
0.0510
0.0596
_. 0.0705
0.0831
0.0964
	 0.1226
                   429

-------
            SAMPLE:  EXC-3
    REL P

    0.1478
    0.1853
    0.2228
    0.3353
    0.4478
    0.5604
    0.6729
    0.7854
    0.8979
    0.9880
VOLUME

0.4228
0.4291
0.4338
0.4453
0.4553
0.4634
0.4707
0.4780
0.4857
0.4925
     S    752.8
     C     -19.881
     R  0.9983
PORE RADIUS
     VOL
1000..
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
. 500.
400.
300.
-—200*.
150.
100.
-. .... . 90.
80.
70.
... 60.
50.
45.
	 40.
35.
30.
25.
20.
18.
16.
14.
12.
--•- 10.
. ... -0.0006
0.0004
0.0007
0.0015
0.0016
0.0032
0.0011
0.0014
0.0018
0.0024
0.0034
0.0024
- ~~ 0.0030-
0.0039
0.0050
, 0.0070
0.0113
0.0071
- 0.0096
0.0119
0.0142
	 -.._ 0.0202-
  CUMV

 0.0006..
 0.0010
 0.0017
-O..0032-
 0.0048
 0.0079
 0.0090
 0.0104
 0.0121
 0.0145.
 0.0179
 0.0203
-0.0233-
 0.0272
 0.0322
 0.0391
 0.0504
 0.0575
 0.0671
 0.0790
 0.0933
 0.1135
                    430

-------
              SAMPLE:  EXD-1
    REL- P
    0.1860
    0.2237
    0.3366
    0.4496
    0.5626
    0.6755
    0.7885
    0.9015
    0.9919
VOLUME.

0.0769
0.0792
0.0818
0.0896
0.0964
0.1019
0.1072
0.1121
0.1176
0.1236
     S    158.4
     C—-.  -37.043
     R  0.9995
PORF RADIUS
     VOL
CUMV
* v >^ v* »
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
400.
300.
	 200. 	 	
150.
100.
	 90. 	
80.
70.
60. -.-..
50.
45.
40.
35.
30.
25. .,
20.
18.
16.
14.
12.
10.
0.0009
0.0004
0.0007
0.0013
0.0012
0.0024
0.0008
0.0010
0.0012
0.0017
0.0024
0.0016
o_no ?o
\J % \J \J *-~ v
0.0026
0.0035
0.005 1
Vr 
-------
           SAMPLE EXH-1
REL P
VOLUME-













PORE
1000.
500.
400.
300.
200.
150.
100.
90.
BO.
70.
60.
50.
45.
40.
35.
30.
25.
20.
IB.
16.
14.
12.
0.1484
0. 1860
0.2237
0.3366
0.4496
0.5626
0.6755
0.7H85
0.9015
0.9919
S 721.
C -19
R 0.9984
RADIUS
500.--
400.
300.
..... 200.
150.
100.
- 90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.4065
0.4106
0.4156
0.4278
0.4383 -
0.4471
0.4544
0.4619 	
0.4696
0.4781
7
.848 - 	 -~- -----

vot
	 -0.0014
0.0006
0.0010
0.0018 	
0.0017
0.0032
O.OOU
0.0013
0.0017
0.0023
0.0034
0.0025
0.0031 	
0.0040
0.0049
0.0069
0.0121
0.0078
0.0102
0.0127
0.0150
0.0192
                           CUMV

                          0.0014
                          0.0021
                          0.0030
                          0*0048
                          0.0065
                          0.0097
                          0.0108
                          0.0121
                          0.0138
                            0162
                            0196
                            0220
                          0.0251-
                          0.0291
                          0.0340
                          0.0409
                          0.0531
                          0.0608
                          0.0711
                          0.0837
                          0.0987
                          0.1179
                432

-------
         SAMPLE:  EXN-1
    REL  P      VOLUME
0. 1426
0.1788
0.2151
0.3237
0.4321
0.5409
0.6495
0.7581
0.8667
0.9753
0.1570
0.1603
0.1638
0.1721
0.1791
0.1850
0.1900
0.1944
0.1996
0.2074
     S    302.4
     C     -26.573
     R.  0.9988
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
10.
0.0015
0.0007
0.00 10
0.0017
0.0016 .
0.0028
0.0009
0.0011
0.0013
0.0017
0.0024
0.0016
0.0018
0.0023
0.0031
0.0049
0.0083
0.0052
0.0068
0.00 86
0.0103 -
0.0148
0.0015
0.0022
0.0032
0.0049
0.0065
0.0093
0.0102
0.0112
0.0126
0.0143
0.0167
0.0182
0.0201
0.0224
0.0255
0.0304
0.0388
0.0440
0.0508
0.0594
0.0697
0.0844
                433

-------
         SAMPLE:  EXV-1
    REL  P
VOLUME
0.1428
0.1769
0.2149
0.3231
.0.4313
0.5395
0.5477
0.7559
0.&641
0.9722
S 667.4
C- -22.
R 0.9985
0.3628
0.3636 .
0.3733
0.3851
0.3950
0.4031
0.4103
0 . 4 1 6.8
0.4242
0.4350
«
544 	
•
PORE RADIUS
     VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500. '
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
Id.
16.
14.
12.
10.
0.0022 .
0.00.09
C.0014
0.0024
0.0022-
0.0040
0.0012
0.0015
0.0019
0.0025
0.0034
0.0023
0.002H
0.0035
O.C047
O.OOfO
0.0115
0.0071
0.0096
0.0123
0.0149 '
. 0.0204
. 0.0022
0.0031
0.0045
0.0070
0.0092
0.0131
- 0.0144
0.0159
0.0178
0.0203
C.0237
0.0260
0.0238
0.0323
0.0369
0.0439
0.0554
0.0625
0.0721
0.0844
0.0994
0.1198
          434

-------
                       APPENDIX A-16
        EXPERIMENTAL RESULTS OF BENCH SCALE RECYCLE
   TESTS - SOLVENT EXTRACTION VERSUS HYDROGEN TREATMENT
1.   S02 Sorption Results from 1" Diameter Fixed Bed      436
      for (NH4)2S Extracted and H2S Generation
      Carbon Samples

2.   S02 Sorption Results from Differential Rate          448
      Apparatus for (NH4)2S Extracted and H2S
      Generation Carbon Samples

3.   Sulfur Generation from 1" Diameter Fixed Bed for     453
      (NH4>2S Extracted and H2S Generation Carbon
      Samples

4.   (NH4>2S Extraction Experimental Results              462

5.   Pore Volume Distribution Runs for (NH4>2S            468
      Extracted and H2S Generation Samples after
      Sixth Cycle
                            435

-------
                        APPENDIX A-16-1

    S02 SORPTION RESULTS FROM 1"  DIAMETER FIXED BED
        FOR (NH4)oS  EXTRACTED AND  H2S  GENERATION
                        CARBON  SAMPLES
                 S02 SORPTION  RATE
                                             8  31 71
RXT-6-1A
JENPFRATURE  =_ 2p8.00QOOO_F	
SPACC VELOCITY «    0.299939E  0~4
INLET S02  MOLE FRACTION (DRY)  =
                               /HR
                                 0.002760
INLET H20 MOLE  FRACTION «__ _.Q.0.9997.8._	.
INLET OXYGEN  HOLE FRACTION =    0.035403
INLET C02 MOLE  FRACTION =    0.0
INLET NO KOLE FRAt.II.ON = „__ 0.000149
INLET INERT GAS MOLE FRACTION =    6.861992
INLET CARBON  WEIGHT =   40.000000 GMS
J.OTAL..GAS. J.COW _=	._7.0.61549_5.CFH	
               (WET) =
           0.0024H4
  TIME
           MOLE FRACTION.S02.
H2S04 LOADING
CMS ACID/GM C
RATE OF  H2S04 SORPTION
   GMS ACID/GM C-MIN
0. .
30.
60.
90.
120.
150.
. 180. _ .
210.
240.
_..260. . ._
0. M!>000t-0.*
0.315000E-03
0.396000E-03
._ 	 0..450000E.-03. 	
0.660000E-03
0.660000E-03
0.600000E-03 _
0.750QOOE-03
0.920000E-03
0.900000E-03
O.u
0.241539E-01
0.478977E-01
0.709748E-01
0.927576E-01
0.113503E 00
0.134545E 00
0.155143E 00
0.174160E 00
...0.186343E. 00
O.U
0.805129E-03
0.777798E-03
0.760674E-03
0.691522t-03
o.egisi'ZE-oj
0.711279E-OJ
0.661885E-03
0.605905E-03
0.612491E-03
AVERAGE  RATE OF S02 SORPTION
                                0.705465E-03
                                436

-------
                   S02 SORPTION RATE
                                    8 31 71
 RXT-6-2A
 TEMPERATURE  =  209.000000 F              _
"SPACE  VELOCITY =    0.299961E 04"/HR	~
 INLET  S02 MULE FRACTION (DRY) =    0.002760
 INLET  H20 MOLE FRACTION *    0.100021
 INLET  OXYGtN MOLE  TRACTION =    0.035045
 INLET  C02 MOLF FRACTION =    0.0
 INLET  NO HOLE FRACTICN =    0.000)50
 INLET  INEK1  GAS MOLE FRACTION =    0.862302
 INLET  CARPON WEIGHT =   29.899994  GMS
 TOTAL  GAS FLOW =    5.278689 SCFH
                                      (W6T) =
                           0.002484
   TIME
     0
    30
    60
    ?.P
   120
   150.
MOLE FRACTION S02
H2S04 LOADING
GMS ACID/GM C
RATE OF II2S04 SORPTIC.N
   GMS ACID/GM C-I-'1N
0.150000E-03
0.150000E--03
0.510000E-03
0.690000E-03
"0.102000E-0?"" 	
0.100500E-02
0.108000E-02
0.120000E-02
0.0
0.257a'tf»E-01
0.497908E-01
0.711296E-01
0.699^030-01
0. 107213E 00
0.124180E 00
0.140185E 00
0.0
0.859484E-03
0.740934E-03
	 0.681660E-03.
f\ K i "\f\ n i™» i~ ^ "»
Wft^i£.'^"w V_*
0.57/929E-03
0.55J231t-03
0.513715E-03
  210
 AVERAGE,RATE  OF  S02 SORPTION =
                       0.642B48E-03
                          437

-------
                    S02 SORPTtON RATE
                                    8 31 71
  RXT-6-3A
	TEMPERATURE =  199.000000 F _	
  SPACE Vl:i.OCitY *    0.299982E O'l /HR
  INLET S02 HOLE FRACTION (DRY) =    0.002780
iiJNLCT H20 MOLE FRACTIQM =.  .  0.100036	
  INLET OXYGEN MOLE FRACTION =    0.034975
  INLCT C02 MOLE FRACTION =    0.0
  INLIT NO fOLE FRACTIUN =    0.000150
  INLET INERl GAS MOLE FRACTION =    0.862338
  INLUT CARBON WEIGHT =   30. 11999!> CMS
  TUTAL GAS FLOW =    5.3180.99 SCFH  _     _
                                      (WET)
                           0.002502
    TIME
MOLE FRACTIOM S02
H2S04 LOADING
GMS ACID/GM C
RATE OF H2SO't SORPTIO^
   CMS AC10/GM C-I-'.IN
_ -. 0. ...,.
30.
60.
90.
, 120.
150.
. .lap, ..
210.
240.
0.270000E-03
0.270000E-03
0.420000E-03
0.585000E-03
«,. 780nnoe-0*
0.1035006-02
0.102000E-02
0.916000E-03
0.885000E-03
0.0
0. 2^79796-01
O.A88546E-01
0.7U557E-01
0.920782E-01
0..110576E 00
0.127892E 00
0.145794E 00
0.164363E PO
0.0
0.82659BC-03
0.777199E-03
0.722862E 03
0.65B644e-03
&.574667E-03
0.579607E-03
0.613856E--03
0.624065t-03
  AVERAGE  RATE  OF  S02  SORPTION =
                       0.672186E-03
                           438

-------
                   S02 SORPTtON RATE
              8 31 71
 RXT-6-4A
 TEMPERATURE =_  204.000000 F 	   _
 SPACE  VELOCITY  =    0.299933E 04 "/MR
 INLET  S02 MOLE  FRACTION (DRY) =    0.002780
 INLET  H20 MOLE  FRACTION =    0.100043
 INLET  OXYGEN MOLE FRACTION =    0.034948
 INLET  C02 MOLE  FRACTION =    0.0
 INLET  NO fOLE FRACTION =    0.000150
 INLET  INERT GAS MOLE FRACTION ' ="    0.862364
 INLET  CARBON WEIGHT =   29.500000  GMS
 TOTAL  GAS FLOW  =    5.207779 SCFH
                (WET)
           0.002502
   TIME      MOLE FRACTION S02
     0. _      0.120000E-03
    30.        0.120000E-03
    60.        0.570000E-03
    90.     _  0.750000E-03
   120.        0.764000F-03
   150.        0.930000E-03
	180.   	0.1Q3500E-02	
•   210.        0.120800E-02
   240.        0.120800E-02
   270.        0.1275006-02
   290.        0.135000E-02

 AVERAGE  RATE OF S02 SORPTION =
H2S04 LOADING
GMS ACIO/GM C

 0.0
 0.262754E-01
 0.503282E-01
_0.712694E-P1
 0.912524E-01
 0.110346E 00
 0.128102E 00
 0.144485E 00
 0.160013E 00
 0.175210E 00
 0.184874E 00

 0.616974E-03
RATE OF H2S04 SORP1ION
   GMS ACIO/GM C-MIN

 	0.0
     0.875846E-03
     0.727676E-03
     C.668408t-03
     0.663799E-03
     0.517605E-03
     0.517605E-03
     C.495544E-03
     0.470849E-03
                        439

-------
                   S02 SORPTION RATE
                                                 8 31 71
RXT-6-5A

TEMPERATURE  =  206.000000 F 	
SPACE  VELOCITY =    0.299917E 04 /HR
INLET  S02  MOLE FRACTION (DRY) «     0.002780
INLET  1120. MOLE FRACTION. =	Q.*_LQ.0.0.26_.		
INLET  OXYGEN MOLE FRACTION =    0.035019
INLET  C02  MOLE FRACTION =    0.0
1NLLT  NO MOLE FRACTION =.    O.OOOIVJ.
INLET  INERT  GAS MOLE FRACTION =     0.862311
INLET  CARBON WEIGHT -   29.279999 CMS
.TOTAL  GA.S . FLOW =	5..168670_._$.CJH _  	
                                                              0.002502
  TIME . __   MOLF  FRACTION S02
                                  H2SO't  LOADING
                                  CMS  ACIO/GM C
                RATE OF  H2SOA
                   GMS AC1U/GM C-HI'N
    0.
   30.
   60.
   90,
  120.
  IbO.
  210.
  240.
  270.
  300.
  320.
              0.270000E-03
              0.270000E-03
              0.720000E-03
          	D.87.0000E.-Q3-
              0.107000E-02
              0.105000E-02
          	Q..1.0.3.5 0.0 E-Q2_
              0.117000E-02
              0.135000E-02
          	0..1A2500E-02.
              0.150000E-02
              0.150000E-02
0.0
0.247928E-01
O.A73632E-01
0.669702E-01
0.0
0.82642BH-03
0.678264E-03
 0.102332E 00
.0_«JL19A94E_P.O..
 0.136064E 00
 0.151078E 00
           00
           00
 0.186275E 00
 0*^7'>'»CCH C3»
 0.569610E-03
...0 ..5_7.ft,549E.-_0_3_..
 0.530099E-03
.Q,44614_OE-03..
 6.42l445t-03
 0.421445E-03
AVERAGE RATE  OF  502  SORPTION
                                   0.563127E-03
                            440

-------
                   S02 SORPTION RATE
                                    8 31 71
 RXT-6-6A
_TGMPERATURE_ =  199.000000 F         __   	
 SPACE  VELOC ITY "~=	6729862 1 FT 04 ~/ll~R	
 INLET  S02 MOLE FRACTION (DRY) =    0.002700
 INLET  H20 MOLE FRACTION =    0.100015
"INLET  OXYGEN MOLE FRACTION =    0.034935
 INLET  C02 MOLE FRACTION =    0.0
 INLET  NO MOLE FRACTION =    0.000150
"INLET  INERT GAS MOLE FRACTION" ="   0'. 862405
 INLET  CARBON WEIGHT =   28.500000 GMS
 TOTAL  GAS FLUW =    5.009249 SCFH
                                      UET)  =
                           0.00243U
   TIME
MOLE FRACTION S02
H2S04 LOADING
GMS ACID/GM C
RATE OF H2S04
   CMS ACID/GM C-MIN
0.
30.
60.
90.
120.
150.
180-
210.
240.
270.
280.
0.0
0.0
0.390000E-03
0.780000E-03
0.855000E-03
0.930000E-03
0.108000E-02
0.121500E-02
0.118500E-02
0.12'4500E-02
0.129000E-02
0.0
0.265547E-01
0.5H916E-01
0.719927E-01
0.905072E-01
0.108284E 00
0.124954E 00
0.1'i0223E 00
0.154976E 00
0.169581E 00
0.174277E 00
U.O
0.88&157I>03
0.757301E-03
0.629445E-03
0.604857E-03
0.580270E-03
0.531094C-03
0.4K6tt3ot-ui
0.496671E-03
0.477001c-03
0.462248E-03
 AVERAGE RATE OF S02 SORPTION =
                       0.600290E-03
                        441

-------
                    S02 SORPTION RATE
                                    8 31 71
  RXT-7-1A

 ^TEMPERATURE =  20.6.000000 £	..
  SPACE VELOCITY =    0.299977E 04 /HR
:  INLET S02 MOLE FRACTION (DRY) =    0.002740
L INLET H20 MOLE FRACTION ~ 	0.099965_ 		
  INLET OXYGEN MOLE FRACTION =    6.035398
  INLtT C02 MOLE FRACTION a    0.0
.. INLtT NO MOLE FRACTION =    0.000149
  INLET INERT GAS MOLE FRACTION =    0.862024
:  INLET CARBON WEIGHT =   40.000000 GMS
,_ryiAL GAS_rLOw =    7.062449 S.CFH	:_
                                      (WET>
                           0.002466
    TIME
MOLE FRACTION S02
H2S04 LOADING
GMS ACID/GM C
RATE OF H2S04 SORPTION
   GXS ACIO/GN C-MIN'
.0.150000C— 03
0.150000E-03
0.210000E-03
0.300000E-03
0.330000E-03
0.345000fc-03
0.570000E-03
0.600000E-03
0.750000C-03
0.0
0.255899E-01
0.508834E-01
0.754359E-01
0.993956C-01
0.123133!: 00
0.145685E 00
0.166977E 00
0.183979E 00
0.0
0.852998E-03
0.8:j3237E-03
0.803596E-03
0.79Jl7l6t-03 """
U. /bH/Yt-t-03
0.714674E-03
0.704793E-03
0.655392E-03
:!: AVERAGE RATE OF S02 SORPTION =
                       0.770802E-03
                           442

-------
                   S02 SORPTION RATE
8 31 71
 RXT-7-2A
.TEMPERATURE =  203.000000 F
 SPACE  VELOCITY" = ~r~ b.299962'E~ "oV/HR	~
 INLET  SU2 MOLE FRACTION (DRY) =    0.002760
.INLET  H20 HOLE FRACTION =    0.099964
 INLtT  OXYGLN MOLE FRACTION =    0.034952
 INLET  C02 MOLE FRACTION =    0.0
 INLET  NO KOLE FRACTION =    0.000150
 INLET  INER1 GAS MOLE FRACTION =    0.862't!>2
 INLET  CARBON WEIGHT =   32.409988 GMS
 TOTAL  GAS FLOW =    5.722059 SCFH
  (WET)  =
O.C02't84
J I ME
0.
30.
60.
90.
120.
150.
180.
210.
240.
••270.
300.
330.
360.
390.
420.
A 50.
480.
4B5.
'ERAG
	 MOLE FRACTION S02
0.138000E-02
0.138000E-02
0.158500E-02
'.'. 0.163500E-02
0.174000E-02
0.186000E-02
0. 180000E-02
0.16650QE-02
0.162000E-02
0.166000E-02
0.177000E-02
0.166500E-02
0.165000E-02
0.180000E-02
0.186000E-02
0.198000E-02
0.204000E-02
0.202000E-02
E~R ATF"OF '1'02~ SORPT fON
H2SOA LOADING RATE OF H2SOA SORPTION
GMS AC1D/GM C GKS AC ID/ CM C-M1N
0.0 0.0
0.136341E-01 0.454471E-03
0.2625b6E-01 0. 3869!>9t-03
0.376173E-01 _ 0. 370492E-03
0.482134E-01 0. 33591 3t-03
0.576980E-01 0. 296394F-03
0.660062E-OI 0. 31ol54E-03
0.770376E-01
0.880783E-01
0.991436E-01
0.109468E 00
0.119768E 00
	 0.130660E.OQ 	
C.140886E 00
0-150074E 00
0.158373E 00
"""O. 165783'E 00
0.166985E 00
0.337610E-03
0.360613t-03
0.375432E-03
0.362259E-03.
0.326033E-03
0.360613E-03
0.365552E-03
0.316154E-03
0.29639AE-03
C.25687tjE-03 .
0.237115C-03
0.243702E-03

                           443

-------
                  S02 SORPTION  RATE
                                     8  31 71
RXT-7-3A

TEMPERATURE_= _ 20.^.000000. F	„	
SPACE VELOCITY =    0.299944E  0'*  /MR
INLET S02 MULE FRACTION  (URY)  *     0.002780
INLCT H20 MOLE FRACTION  =  __Q_._lOOpfi5	:
INLET OXYGF.N MOLE FRACTION =    0.035078
INLET co2 MOLE FRACTION  =    o.o
INLET NC MOLE FRACTION =   0.000149
INLET INERT GAS MOLE  FRACTION  *     0.862216
INLET CARBON WEIGHT =    27.289993 GMS
TOTAL GAS FLOW =    4.8 17.819__SC,FH.	
                                       (WET)  -
                            0.002502
  TIME
    0. . _
   30.
   60.
   90. _
  120.
  150.
  1 HO -   _
  210.""
  240.
 ..27Q._	
  300.
  330.
 -360.	
  390.
  420.
 __450.	
  480.
  510.
 .^520.		
MOLE FRACTION S02
  0.117000E-02
  6.117000E-02
  O.l'tlOOOE-02
  0.144000E-02
  0.153000E-02
  0.168000E-02
  h, l is?OOr>F-0?
  0.180000E-02
  0.177000E-02
  0.186000E-02
  0.194000E-02
  0.188500E-02
  .0.187000E.T02_
  0.195000E-02
  0.196500E-02
  0.189000E-02.
  0.196500E-02
  0.208000E-02
  0.2100.0QE-02,
H2S04 LOADING
GMS ACIO/GM C
RATE OF H2S04  SORPTICN
   GMS 'ACID/GM C-KIN
0.0
0.159041E-01
0.306227E-01
0.440078E-01
0.568002E-01
0.684072E-01
0.795696E-01
0.901394E-01
0.999683E-01
0.109501E 00
0.118194E 00
0.126763E 00
	 , 	 .0... 135.6.7.8 E. .00..
0.144272E 00
0.152397E 00
0.160818E 00
0.169240E 00
0.176722E 00
- 	 _. 0.,. 1.7 3 9 9.4 E. 00
0.0
0.530136E-03
0.451109t-Q3
0.441231E-03
0.411596E-03
0.362205E-03
0.381961E-03
0.3226911: -03
0.332569E-03
0.302935E-03
C.276593E-03
0.294703E-03
672 7 3 300 E - 0 3
0.268361E-03
C.293056E-03
0.268361E-03
0.230494E-03
0.223908E-03
AVERAGE RATE OF S02 SORPTION
                       0.335513E-03
                          444

-------
                  $02 SORPTION  RATE
                                    8 31 71
RXT-7-4A
TEMPERATURE =  202.000000  F
SPACE VELOCITY =    0. 299954E~"~04  /HR  "
INLL-T 502 MOLE FRACTION  (URYJ  =    0.002780
INLET H20 MOLE FRACTION  =     0.100010
INLET OXYGEN MOLE  FRACTION =    0.034786
INLET C02 MOLE FRACTION  =     0.0
INLET NO MOLE FRACTION =   0.000149
INLET INERT GAS MOLE FRACTION  =    0.862560
INLET CAKUUN WEIGHT =    24.750000 GMS
TOTAL GAS FLOW =    A.369549  SCFH
                                      (WET) =
                           0.002^02
  TIME
MOLE FRACTION S02
H2S04 LOADING
GMS ACIO/GM C
RATE OF II2S04 SORPTION
   GMS ACID/GM C-I'.IN
:".. 0 .
30.
60.
90.
1 120.
'• iyO.
. 180.
210.
240.
270.
; 300.
330.
360.
390.
420.
450.
480.
510.
540.
570.
0.135000E-02
0.135000E-02
0.167000E-02
0.180000F:-02
0. 186000E-02
0* i*' >OvV^u"" O" C.
0.186000E-02
0.195000E-02
0.192000E-02
0.201000E-02
O.183000E-02
0.171000E-02
0.165000E-02
0.165000E-02
0.156000E-02
0.162000E-02
0.162000E-02
0.192000E-02
0.200000E-02
0.200000E-02
0.0
0.141270E-01
0.266733E-01
0.369969E-01
0.463819E-01
0.5502COC-C1
0.636702E-01
0.723143E-01
0.806620E-01
0.887133E-01
0.972093E-01
0.107187E 00
0.1180'34E 00
0.129217E 00
0.140825E 00
0.152581E 00
0.164041E 00
0.174018K 00
0.182119E 00
0.189825E 00
0.0
0.470900t:-03
0.365524E-03
0.322714E-03
0«3029t)6E-03
n •> 7 J 7 I o c — r> i
0.302956E-03
0.273319E-03
0.283198E-03
0.253561E-03
0.312835E-03
0.352351E-03
0.372110E-03
0.372HCE-03
0.401747E-03
0.38L989E-03
0.381989E-03
0.2H3198E-03
0.2b6n54e-03
0.2')6b54fc-03
AVERAGE RATE OF S02 SORPTION
                       0.327393E-03
                         445

-------
                   S02 SORPTIQN RATE
                                                8 31 71
 RXT-7-5A

 TEMPERATURE  =__?03.000QQp_JF	,_
 SPACE  VELOCITY =    0.299947E 04 /HR
 INLET  S02  MOLE FRACTION IUE_-JQ1...
  0.9A8716E-01
  0.103639E 00
  0.1102>9E 00
  0.116335E 00
  0.121744L 00
.__0.126.700F 00
  0.131228E 00
  0.135452E 00
  0.139602E 00
  0.144047F 00
  0.148493E 00
	0_.J..52.7.9IE 00
  0.157015E 00

  0.206751t-03
RATL-
  : H2S04
  ACID/OK C-NIN
0..0
0.263462E-03
0.24b995E-03
0.276635E-03
0.246995E-03
0.2272.36^-03
0.256875E-03
0.227236E-03
0.204183E-03
0.246995E-03
0.246995E-03
0.263462.t-03
0.2272.36E-03
0.223942E-03
0.217356E-03
0.1fi7717E-03
0. 172097E-03
0. l^^07tE-0^_
0.143257L-03
0. 13U317L-03
0.13BJ17L-03
0. 15 HO 7 71: -03
0.138317C-03
0_. 14U197C-03
0. 133378F-03
                         446

-------
                  S02 SORPT10N RATE
             8 31 71
RXT-7-6A
TEMPERATURE = 203.000000 F
SPACE VELOCITY *" 0. 299986E
INL1IT 5112 MOLE FRACTION (DRY)
INLET H?0 MOLE FRACTION =
INLET OXYGEN MOLE FRACTION =
IMLET C02 MOLE FRACTION =
INLET NO MOLE FRACTION = 0
INLET INERT GAS MOLE FRACTION

04 /HR
- 0.002760
0.099932
0.014928
0.0
.000150
0.862bl7


(WET) = 0.0024K-'.





INLET CARBON WEIGHT = 23.349991 CMS
TOTAL GAS FLOW = 4.122819
	 TIME _.MOLE FRACTION .502

0. 0. 163500E-02
30. 0.163500E-02 	
60. 0.171000E-02
90. 0.192000E-02
,-j. 120. 0.198000E-02
? 150. 0.204000E-02
ISO. 0. 1950CCE- 02
210. 0.198000E-02
240. 0.201000E-02
270. 0.213000E-02
i: 300. 0.207000E-02
: 330. 0.211000E-02
345. 0.210500E-02
360. 0.210000E-02
390. 0.216000E-02
420. 0.1.95000E-02
! 450. 0.205000C-02
* 480. 0.207000E-02
__ 510. 	 .0..2.15QOOE-02 	
540. 0.19500QE-02
570. 0.195000E-02
600. 	 0.206000E-02
630. 0.204000E-02
660. 0.210000E--0.?
690. 0.207000E-02
710. 0.207000E-02
SCFH
H2S04 LOADING
CMS ACID/CM C
0.0
O.lll 160E-01 '
0.218615E-01
0.311990E-01
0.392026E-01
0.466133E-01
0.5*,1722E-01
0.620275E-01
0.695064E-01
0.764042E-01
0.829256E-01
0.695458E-01
0.927694E-01
0.96017BE-01
0.102243E 00
0.109209E 00
0.116718E 00
0.123635E 00
0.130057E 00
6.137073C 00
0.145076E 00
0. 152-5366 00
0.159552E 00
0.166370E 00
0.173039E 00.
0.177584E 00

RATE OF H2SO'( SOKPTION
CMS AC1U/GK C-J'IN
	 0.0
0.370535E-63
0.345832E-03
0.2/6666E-03
0.2'.>6904E-03
0.237142F-03
0.26t7S5i'-03
0.256904E-03
0.247023E-03
0.207'50CE-03
G.22/26H--03
0.214087E-03
0.215734E-03
0.217381E-03
0.197619E-03
0.266785E-03
0.233849E-03
0.227261E-03
_0.200912E-03
0.26f>785t--OJ
0.266785L-03
0.2305'55E-03
0.237142E-03
0.217381E-03
0.227261E-03
0.227261E-03
AVERAGE RATE OF 502 SORPT10N
0.24705/E-03
                           447

-------
                   APPENDIX A-16-2
   SOo  SORPTION  RESULTS  FROM DIFFERENTIAL RATE
     APPARATUS FOR  (NH4)2S EXTRACTED AND H2S
              GENERATION CARBON  SAMPLES
                    GRAVIMETRIC FLOW EXPERIMENTS
Run:       180-G          SO?.:
Dry Weight:  95.10 mg        NO:
Deflection:  -6.18 mg.       02=
Carbon:     Virgin,         HgO:
            C-70-7T
2000 ppm
150 ppm
3.5#
6.055
          200°F
          1500 cc/min.
          75.11*
Correction:  0.1(907
Date:      August 3, 1971
Time
minutes
1
2
3
It
5
6
7
8
9
10
12
1>)
16
18
20
?5
30
35
1)0
1)5
50
60
70
80
90
100
330
120
330
11)0
150
360
170
180
190
200
230
2?P
230
2')0
250
260
270
280
290
300
Load
mg. HpSOlj/g. C
ll).72
37.35
39.35
20.93
22.08
23.fl)
2l) . 1(0
25.55
26.71
27.87
29-97
32.07
3l).17
36.38
38 . 1)9
Itl4.36
iio.aii
55.1)2
61.20
66.88
72.55
83.70
95-06
106.1)1
33.7.67
128 . 39
130.80
31)9.21
159-52
]6o.liO
379.18
380.06
198.32
207.36
215.77
223.76
231.1)1)
239.32
?1)6.27
253. 1(2
260.36
266.93
273-50
279.81
285.91
291.90
Mean Load
mg. HgSOlt/g. C
6
8
10
12
ll)
16
18
20
25
30
35
1)0
1)5
50
55
60
65
70
75
80
85
90
95
100
110
120
130
ll)0
350
160
170
180
190
200
220
2l)0
260
280
300







Rate
HIR. H2S01t/g. C/min.
36.21)63
13.9327
11. 63 93
9.1(637
6.5720
3.2597
1.8822
1.5563
1.1672
1.0726
1.0726
1.1251
1.1356
1.1356
1.11)62
1.1567
.1 . 1 567
1.1567
1.1567
1.1567
1.1567
1.1567
. l.ii)62
1.11)62
1.1251
1.1 oia
1.0936
3.0726
1.0515
1.0305
1.0095
0_.9881)
0.9569
0.9253
0.8623
0.7886
0.7150
0.6309
0.51)68







                             448

-------
                          GRAV1MKTK1C FLOW
Run:         185-G
Dry Weight:   97.2U mg.
Deflection:   -5-9^ me-
Carbon:      RXT-6-3C
S02:
NO:
02:.
"20:
2000 ppm
150 ppm

6.07,
t:
Ft:
% IIpl.'Ol.:
Correction :
Date :
200°F
1500 en /win.
77-72
0.5076
August 20, 1971
Time
minute's
1
V
3
)i
c;
(>
7
8
9
10
12
Hi
16
18
20
25
OA
35
1(0
'(5
50
60
70
80
90
100
1.10
120
a 30
]1|0
350
160
170
100
190
POO
210
220
230
2'iO
250
260
2?0
?80
290
300
Load
mf,. }If>t:oj,/p:. C
5.55
8.6)-i
11 .00
1.3.27
J 5 . 3?
17. OY
18.9;'
20.57
22.21
23.76
26.1i3
29.21
31.78
3l*. 25
36.71
1)2.37
':7 . 72
52.55
57.28
61.81
66.23
7^.56
82.68
90.60
98.72
106. 6li
1 Hi. 66
12?. it 8
130.19
:i 37 • 70
I'i5.?.l
152. 'it
159-30
166. :i 9
173.08
179.86
186.65
193. '»li
199-9?
206 . 50
212.67
218.63
22'i.6o
230. !) 6
236.3''
21(1.88
Moiui Load
mg. Up;:/)],/,";. C
2
1|
6
8
'1 0
1?
Ill"
16
1H
20
25
30
35
)|0
'*5
50
rr
s s
60
65
70
75
80
85
90
95
100
110
120
130
ihO
150
360
170
l8o
190
200
220
2*40



•




Rate
rn.'-. Hp:/i)|/r:. 0/min.
5.01(12
it. 7306
3.77>42
3.":',37
2.1..V)P
2. fill)
2. 00 '".3
1.851-1
1.7277
] .621(8
1.1(500
1.3318
1.2230
1.1261
1.01490
0.9821
0.9255 ~"
0.8896
0.8536
0.8381
0.8227
0.812)4
0.8073
0 . 8021
0.7970
0.7970
0.7919
0.776*1
0.7610
0.7*156
0.7302
0.71)17
0.69)1?
0.6736
0.6582 •
0.61(27
0.5965
0.5502








                              449

-------
GRAVIMETRIC FLOW EXPERIMENTS
Run:         1B6-G
Dry Weipht:   101-70 mg.
Deflection:   -6.35 mg.
Carbon:      RXT-7-3C
     NO:
     H20:
2000 ppm
150 ppm
3.5%
6.0%
t:
Ft:
             200°F
             1500 cc/min.
             75-56
Correction:  O.li93li
Date:        August 23, 1971
Time
minutes
]
2
3
lj
5
6
7
8
9
10
12
• 111
.16
.18
20
25
'.•r>
35
1*0
1*5
50
60
70
80
90
HOG
110
120
330
.1.1)0
150
l6o
170
180
390
200
210
220
230
?1|0
2^0
260
270
280
290
300
Load
mg. H2SOl|/K. C
6.78
8.95
10.ll2
11.50
12.29
12.90
13.67
11*. 36
15 . Ok
15-73
16 .21
18.19
19.'i7
20.55
21.73
2l*.39
27.l'i
29.60
31.96
3l*. 32
36.68
1*0.90
1*5-23
1*9.16
52.90
56.M
60.28
61*. 01
67.1*5
71.1*8
75.22
79.35
83.1*8
87.1)1
91 .05
9k . 59
98.03
101.57
105.53
1 09.W)
113 .27
lif.ll
120 .9'i
121* . 78
128.1)2
131.86
Mean Load
ing. E2SOk/E- C
It
6
8
10
12
1>*
16
18
20
25
30
35
1*0
1(5
50
55
f$n
65
70
75
80
8=5
90
95
100
110
120
130













.




Bate
rag. HgSOli/fl. C/nrin.
5.5261
3.6185
2.26.16
1 . 37^6
0.8505
0.7030
0.6391
0.591*9
0.5605
0.5015
0.1(720
0.1)523
O.Ul25
0.1*277
0.1)228
0 . 1*179
O . 1(1 7Q
0.1)179
0.1*179
0.1*179
0.1)130
O.liOSl
0.1*031
0.3982
0.3933
0.3736
0 . 3589
0.3392


















   450

-------
                          GRAVIMETRIC FLOW  CALCULATIONS
Run:         187-G
Dry Weight:  91.92 ing.
Deflection:  -5-98 mg.
Carbon:      RXT-7-5C
S02:
NO:
02:
HgO:
2000 ppm
150 pj)m
3.5#
6.0?
t:           200°F
Ft:          1500 cc/min.
% H2S01(:     75.83
Correction:  0.1)952
Date:        August 2l), 1971
Time
minutes
1
2
3
1*
5
6
7
8
9
10
12
Ik
16
18
20
25
3n
35
1)0
1*5
50
60
70
80
90
100
110
120
130
ll)0
150
160
170
180
190
200
210
220
230
2)|0
250
260
270
280
290
300
Load
mp. UjjEOij/f-. C
7.29
1.0.K'
ia.97
13.27
in . 1*7
15. >*5
J6.l)3
17-30
18.06
18.71
19-9-1
21.00
22.19
23.39
21*. 1*8
27.09
90. ^0
31.98
33.9'+
36.01
37-86
1)1 .78
!)5.1»7
J)9 - ] 7
52.65
55- 92
59-10
62.66
65.93
68.97
7-1.91
75.17
78.1)1)
81.59
81*. 75
87-79
91.06
9't.-10
97.69
101.07
I0l).33
107.27
109.99
112.92
].15.5lt
117.93
Mean Load
mg. H2BOi,/g. C
1*
6
8
10
12
Hi
.1.6
18
20
25
30
35
1*0
1*5
50
55
60
65
70
75
80
85
90
95
100
110
120














,




Rate
mg. HpSOjj/g. C/trdn.
6.1)730
lt.7868
3.3616
2.T'08)|
1. Ii687
1.1151
0.8975
0.7398
0.636li
0.1*896"
0.1*569
0.')297
0.1*080
0.3916
0.3808
0.3753
0.3699
0.3590
0.3536
0 . 3l*8l
0 . 3372
0.3261)
0.3209
0.301)6
0.29^7
0.2665
0.2393



















                               451

-------
                          GRAVIMETRIC FLOW EXPERIMENTS
Bun:          188-G             S02:
Dry Weight:   100.66 mg.         NO:
Deflection:   -5-96 mg.          02:
Carton:      RXT-6-5C          HoO:
2000 ppra
150 ppm
3.555
6.0%
t:           200°F
Ff.          1500 cc/min.
% H2SOi,:'     76.97
Correction:  0.5027
Date:        August 25, 1971
Time-
minutes
1
'•i
t
3
!j
S
.. . £ . .
7
8
9
.10
12
111
16
18
20
25
on
35
1.0
U 5
50
60
70
80
90
100
:I.LO
120
130
I'lO
150
160
.170
180
J90
200
210
220
230
2lib "
2^0
260
270
2CO
290
300
Load
mg. Il2S01)/R. C
7.15
.10.53
13.31
15-50
37.6(1
19. 5Y
21 . 36
23.15
2>i.7)4
26 . 33
29 . 31
32.39 •
3'i.«7
37-55
liO.Oli
JJ5.90
n:n o£
J.IL. . ..^-
56.'i3
61.10
65.67
70 .Oil
78.1)8
86.83
9'i.87
102.52
109-97
117.23
12l).li8
131.53
138.1)9
I'i5.3l)
1 52 . 39
159.15
365.71
172 . 36
170. ft;1
iSli.ftB
390.611
136.70
202.56
20C.52
?l'i.39
220 . 1 S
225.91
23-1 .27
vtiM
Mean Load
m;-;. HoSOIj/g. C
If
6"
B 	 ~
10
If?
Ill
. 16
18
20
25
30
35
1)0
'15
50
55
f,r\
65
70
75
80
85
90
95
100
110
120
130
lliO
150
160
170
180
190
200
220
?1|0









Rate
mg. HgSOli/g. C/iriiii .
6.3332
li.6U93
3.6956
3.0995
2.6376
2.37^3
2.1111
1.9'i22
.1.8180
1.5895
I.)i355
1.3:i63
1.2170
1.1276
1.01)81
0.993li
0 . 9li3ft
0.9090
O.G7l)2
0.81»9l*
0.8295
0.8lU6
0.79W '
0.7799
0.7699
0.7^51
0.7252
0.7053
0.690i|
0.6706
0.6557
0.6)i57
0.6259
0.61.10
0.591.1
0.5563
0.5166









                                452

-------
                    APPENDIX A-16-3

   SULFUR GENERATION FROM 1 INCH DIAMETER FIXED BED
FOR (NH4)2S EXTRACTED AND H£S GENERATION CARBON SAMPLES
                           453

-------
                                                RATF OF  SULFUR GENERATION
                                                      BtNCH SCALE
 RXT-6-IB

 SPACE VELOCITY =     0.100125E  04  /HR
 INFRT GAS FLOW RATE  =       623.00 SCC/MIN
 i^EIGHT OF CARBON,  UNLOADED  *       32.000 GHS
                                                          LOADED
 INLET PERCENT H2S  ~       38.000
 INLET MOLAR H2S CONCENTRATION  -
 INLET SULFURIC ACID  LOADING  =
                                           0. 612903 MOLES H2S/MO_Lt
                                         0. 1137600 CMS H2S04/GM CARBON,
                                                       l.68
_*P_-JLP.GMS


 GAS
        FINAL OUTLET PERCENT SULFUR LOADING ON CARBON =	  	
4S      FINAL OUTLET SULFUR LOADING ON CARBON =    "  0.248~GMS S/GM CARBON
Ui      INITIAL TEMPERATURE =      270.00 F
-!>•      MAXIMUM TEMPERATURE =	315.00 F	
      "FINAL TEMPERATURE =      310.00 'f
                                                                                            8  31  71
PERCENT S02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
PERCENT CO2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
MOLAR CONC H2S
0.0
0.214505E-01
0.219512E 00
0.199041E 00
0.319261E 00
0.562500E 00
0.612903E 00
0.612903E 00
H2S04 LOADING
GMS ACIO/GM C
0.187600E 00
0. 102135E 00
0. 322466E-01
-0.250390E-01
-0.752A60E-01
-0.996606E-01
-0.103237E 00
-0*!03237E 00
RATE ACID DECOMP.
GM ACIO/GM C-KIN.
0.0
-0.167B86E-01
-0.111666E-01
-0.1174776-01
-0.833515E-02
-0.143072E-02
0.0
0.0
 TIME     PERCENT H2S
   0.0    0.0
   5.0    0.2100006 Oi
	10.0	0.180000E 02
  15.0    0.166000E 02
  20.0    0.242000E 02
 _25.0    0.360000E 02
  30.0 " 0.380000E 02
  35.0    0.380000E 02

 ACID LOADING -    0.1876bOE»01 AT0.111771E 02 MINUTES
 RATE OF  ACID DECOMPOSITION »   -0.113034E-01 AT    0.111771E 02. MINUTES
 AVERAGE  RATE OF ACID DECOMPOSITION UP TO 90_PERC_ENT ACID UTILIZATION =
                                                                                 -O.I5696CE-01

-------
Ul
Ul
                                                       RATK OF  SULFUK  GENEKAHUN
                                                              BENCH  SCALE
                                                                                       ri  31  71
       RXT-6-2B
       SPACE VELOCITY  =     0.500870E 03 /HR
       INERT GAS  FLOW  RATE  »      291.00 SCC/NLN
      _ME|GHT._QF. CARBON,  UNL QA.D JE D_2	29.900 CMS
                                                    LUADEO
33.61 GMS
       INLET PERCENT  H2S ^      32.000
       LNLE_T_MOLAR_ H2S CONCENTRATION =
       INLET SULFURIC *CID LOADING »
                                     Q.47058B HOLES H2S/MOLE INERT GAS
                                   0.139600 GMS H2SQ4/GM CARBON,
 FJNAL Oj^f).EX.I^RGEN.T'SULFUR  LQA01NG ON CARBON
 FINAL OUHET, SULFUR  LOADING  ON  CARBON -
 INITIAL TiHP€RATURE  *      280.00 F
JLAXIMUM TEMPERATURE.;	300.00 F	
 FINAL TEHPERATURE =       298.00 F
                                                              15.420
                                                      0.184  GMS  S/GM  CARBON
       TIME
          PERCENT H2S
PERCENT S02 PERCENT C02
0.0 .
0.0
0.0
0.0
0*0
O.O
0.0
0.0
0*0
0.0
0.0
0.0
MOLAR CONC H2S
0.0
0.140251E
0.216545E
0:2903236
0.470588E
0.470588E
00
00
00
00
00
H2S04 LOADING RATE ACID DECOMP.
GMS ACID/GM C GM ACID/GM C-MIN.
0.139600E 00 .
0.827747E-01
, 0.4131326-01
0.104992E-01
-0.229061E-02
-0.229061E-02
0.0
-0.468745E-02
-0.360485E-02
-0.255795E-02
0.0
0.0
                 0.0
                 0.123000E 02
               __0. 178000E__02
                 0.225000E 02
                 0.3200OOE 02
               _._.0.320000E 02

        ACID  LOADING =    0.139600E-01 AT    0.288769E 02 MINUTES      ^    ?
        RATE  OF ACID DECQMPQSLI JON j?	-0_.2J>mM-0_2_ AJL..	a»_28,8769E _Ql_H.LNUTeS
        AVERAGE RATE OF ACID DECOMPOSITION UP TO 90 PERCENT  ACID  UTILISATION
                                                                           -0.369408E-02

-------
Ul
                                                      RATE  OF  SULFUR GENERATION
                                                            BENCH  SCALE
                                                                                    8 31 71
      RXT-6-3B

      SPACE  VELOCITY  =     0.^996025  03  /HR
      INERT  GAS  FLOW  RATE  =   =    293.00 SCC/MIN
      WEIGHT  OP  CAHBONt  UNLOADED =       30.120  CMS
                                                   LOADED
35.95 CMS
       INLET  PERCENT  H2S =      32.500
       INLET  MOLAR  H2S CONCENTRATION^
       INLET  SULFUR 1C AClD LOADING =
                                    0.481481 MOLES H2S/MOUE INERT £&S
                                  0.167100 GMS H2S04/GM CARBON*
 FINAL Ot/TLET PERCENT SULFUR LOADING ON CARBON
 FINAL OUTLET SULFUR LOADING ON CARBON -
 INITIAL TEMPERATURE =      270.00 F
 MAXIMUM 'TEMPERATURE^*	HP_.00_F	
'FINAL TEMPERATURE'-      298.od" r
                                                            17.910
                                                           GMS  S/GM  CARBON
      TIME
          PERCENT H2S
0.0
10.0
20.0
30.0
40.0
50.0
60.0
0.0
0.0
0.250000E 01
0.263000E 02
0.2750006 02
0.310000E 02
0.325000E 02
PERCENT S02 PERCENT C02 KOLAR
0.
0.
0.
0.
O.
0.
0
0
0
0
0
0
0.0
7100E-01 AT 0,,
0
0
0
0
0
0
0
oO
.0
.0
.0
.0
.0
.0
2 MINUJE.S_ 	
0
0
0
0
0
0
0
CONC H2S
.0
.0
.256410E-01
.356852E
.379310E
.449275E
.481481E
00
00
00
00
H2S04 LOADING RATE ACID DECOMP.
GMS ACID/GM C GM AC1D/GM C-MIN.
0
0
0
-0
-0
-0
-C
. 167100E 00
.9881UE-01
.323407E-01
.882351E-02
.249071E-01
— •;•- - -. - - ^ ,^_L-^ 	 — r ------ :
0.0
-0.682888E-02
-0.6465216-02
-0.
-0.
-0.
0.
176763E-02
144910E-02
456781E-03
0
      ACID LOADING =    0      		
      RATE OF ACID DECOMPOSITION  =    -0.468147E-02  AT     0.237971E  02  MINUTES
      AVERAGE RATE OF ACID  DECOMPOSITION  UP  TO 90 PERCENT ACID UTILIZATION  =   -0.633341E-02

-------
                                                 RATE Of SULFUR GENERATION
                                                       BtNCH SCALE
 RXT-6-4B
  SPACE  VELOCITY =    0.500339E 03 /HR
  INERT  GAS  FLOW RATE =      287.00 SCC/MIN
 Jrf.EIGHT.pF  CARBON,  UNLOADED_•	29.500 CMS
                                                        LOADED
36.69 QMS
  INIET  PERCENT H2S =      30.000
  INLET  MOLAR H2S CONCENTRATION =
  INLET  SUtFURIC AC 10 LOADING =
                                         0.428571 MOLES_ H2S/MOLE_LNERJ_GAS_
                                       0.185300 GMS H2S04/GM CARBON,
_F INAL_OUTLET PERCENT,SULFUR LOADING ON CARBON =
Ui    FINAL OUTLET SULFUR LOADING ON CARBON
^J    INITIAL TEMPERATURE »      305.00 f
    _HAXIWUM TEMPERATURE * 	   311.00__f_ ___
      FINAL tEMPERATURE »      297.00 F
                                                           1V.48Q
                                                                                           a  31  71
                                                0.2<»2 CMS S/GH CARBON
TIME PERCENT H2S
-1 M ' '
0.0
15.0
30.0
45.0
60.0
0.0 , , .
0.8500QOE 01
0.223000E 02
0.262000E 02
0.300000E 02
PERCENT S02
0.0
0.0
0.0
0.0
0.0
PERCENT C02
0.0
OeO
0.0
0.0
0.0
MOLAR CONC H2S
0.0
0.928962E-01
0.287001E 00
0.355013E 00
0.428571E 00
H2S04 LOADING RATE ACID DECOMP.
GMS ACID/GM C CM ACID/GM C-MIN.
0.185300E 00 i
0. 103996E 00
0.532245E-01
0.303382E-01
0.225I27E-01
0.0
-0.476142E-02
-0.200812E-02
-0.104339E-02
0.0

-------
                                                       RATF DP SULFUR f.FNFRATION
                                                             BENCH SCALE
                                                                                     8  31  71
-P-
Ul
oo
        RXT-6-5B

        SPACE  VELOCITY =    0.500410E 03 /HR
        INERT  GAS .FLOW RATE *      285.00 SCC/MIN
        NEIGHf'OF'CARBON, UNLOADED =      29.280 QMS
                                                   LOADED,.?.	35._80 GM_S_
        INLET PERCENT H2S =      34.200
        INLET MOLAR H2S CONCENTRATION -
        INLET SULFUR 1C ACID LCiADlNG~~=
                                 	OOE-Ol AT
S02 PERCENT CO2
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.237^58E 02 MINUTES
MOLAR CONC H2S
0.0
0.204082E-01
0.695187E-01
0.43B849E 00
C.497006E 00
0.519757E 00
0.519757E 00
H2S04 LOADING
CMS ACID/GH C
0.186000E 00
0.775295E-01
-0.235415E-01
-0.800750E-01
-0.837527E-01
-0.8^5599E-Oi
-0.8^5599E-01
RATE ACID OECOMP.
GW ACID/GM C-MIN.
0.0
-0.708655E-02
-0.63896CE-02
-0. 114821E-02
-0.322871E-03
0.0
0.0
       ACID LOADING  =     0.1      	
       RATE OF ACID  DECOMPOSITION =   -0.668019E-02 AT    0.237458E 02 MINUTES
       AVERAGE RATE  OF  ACID DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION =   -0.693688E-02

-------
                                                RATE  OF SULFUR GENERATION
                                                      BENCH SCALE
                                                   8 3i 71
RXT-7-IB
SPACE VELOCITY  =     0.494292E  03  /HR
INERT GAS  FLOW  RATE  »       312.00 SCC/MiN
HEIGHT Of  CARBONt  UNLOADED ......   32.410 GMS
                 LOADED
38.60 GMS
INLET PERCENT  H2S  *       26.800
1NLET MOLAR  H2S  CONCENTRATiON =
INLET SUIFURIC ACID~ LOADING "»
  0.366120 MOLES H2J7 MOIE_ INERT GAS
0.167400 GMS H2S04/GM CARBON*
LlJS!AL.OUTLET  PERCENT SULFUR LOADING ON CARBON
FINAL OUTLET  SULFUR LOADING ON CARBON =
INITIAL  TEMPERATURE =      273.00 F
MA_XIMUM  TEMPERATURE _•	303.00 F	
FINAL TEMPERATURE  *      302.00 F      ;
                    17,970
             0.214 GMS S/GM CARBON
TIME      PERCENT H2S
  0.0     0.0
  30.0     0.6500006 01
_60_. Q	Q . 252 OQQ.E_fl2
  90.0     0.256000E 02
 105.0     0.268000E 02
 ACID  LOADING -    0
 RATE  OF  ACID DECOMPOSITION
PERCENT S02
o.o . : •:. .. .•;••••,..•.
L 0.0 :-' .- •:,:-s''-:. :
> 0.0
> 0.0
I 0.0
PERCENT C02 MOLAR CONC H2S
0.0 0*0
0.0 0.695187E-01
0.0 . 0.33689SE 00
0.0 0»?44086E 00
0.0 0.366120E 00
H2S04 LOADING
GMS ACID/GM C
0.167400E 00
0.278739E-01
-0.407232E-01
-0.5151-V3E-01
-0.538338E-01
RATE ACID OECOMP.
GM ACIO/GM C-MIN.
0.0
-0.416300E-02
-0.410U5E-03
-0.30926*E-03
0.0
L67400E-01 AT 0.3A8693E 02 MINUTES
5ITION = -0.355388E-02 AT 0.3^8693E 02 MINUTES
DECOMPOSITION UP TO 90 PERCENT ACID UTILIZATION = -O.A07793E-02

-------
-p-
ON
O
                                                        RATE  OF  SULFUR  GENERATION
                                                              BENCH SCALE
                                                                                     B 31  71
        RXT-7-2B

        ~SPACE  VELOCITY -     0.615268E 03 /KR ~
        INERT  GAS  FLOW RATE  =      315.00 SCC/MIN
        WEIGHT  OF  CARBON,  UNLOADED =      26.330 CMS
                                                   LOADED
32.41 CMS
         INLET  PERCENT  H2S  =      26.300
         INLET  MOLAR  H2S  CONCENTRATION =
         INLET  SULFURIC ACID LOADING «
                                    0.356852 MOLES H2S/MpLE__INERJ_GAS
                                  6.168900 GMS H2S04/GM CARBON,
_FINAL OUTLET PERCENT SULFUR LOADING ON CAK80N
 FINAL OUTLET SULFUR LOADING"ON CARBON =
 INITIAL TEMPERATURE *      270.00 F
 MAXIMUM TEMPERATURE =      315.00 F	
 FINAL TEMPERATURE *      ~300JOO F
                                                              18.070
                                                       0.222  GMS  S/GM  CARBON
        TIME
PERCENT H2S
0.0
0.0
0.0
0.400000E 01
0.230000E 02
0.245000E 02
0.260000E 02
0.255000E 02
0.260000E 02
PERCENT S02
0.0
0.0
0.320000E
0.300000E
0.0
0.0
0.0
0.0
0.0
0.263000E 02 0.0
ING = 0.168900E-01 AT 0
01
00

PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
o.o - •,
0.0 :
0.0
.295749E 02 MINUTES
MOLAR CONC H2S
0.0
0.0
0.0
0.417973E-01
0.298701E 00
0.324503E 00
0.351351E 00
0.342282E 00
0.351351E 00
0.356852E 00
H2S04 LOADING
GMS ACID/GM C
0.168900E 00
0.137777E 00
0.106655E 00
0.480550E-01
0.155062E-01
0.115598E-01
0.990935E-02
0.903412E-02
0.728368E-02
0.704382E-02
RATE ACID OECOMP.
GM ACID/GM C-MIN.
O.O
-0.622
-------
                                                  RATE  OF  SUI FIIK GENERATION
                                                        BENCH SCALE
                                                    8  31  71
  RXT-7-5B

"SPACE VELOCITY =    0.500329E 03 /HR "~     ~'~
  INERT GAS FLOW RATE =      237.00  SCC/MIN
__MilGH.L OF...CARBON»_ UNLOADED =       2*.320 CMS
                ;J  LOADED
30.90 CMS
  INLET PERCENT HZS =      28.000
  INLET MOLAR H2S CONCENTRATION =_
  INLET SULFURIC ACID LOADING -
	0.388889 MOLES H2S/MOLE INERT GAS
 0.18*000 CHS H2S04/GM CARBON*
_JF INAI._.OUTLET _PEJU:ENT SULJUR LOADING  ON  CARBON
  FINAL OUTLET SULFUR LOADING ON CARBON
  INITIAL TEMPERATURE =      270.00  F
  MAXIMUM TEMPERATURE =	  310.00 j
  FINAL TEMPERATURE =      300.00  F
                     19*350
              0.246 CMS S/GM CARBON
TIME
0.0
15.0
_30.0.
60.0
75.0
90.0
105.0
120.0
PERCENT H2S
0.0
0.1000QOE 01
0.800000E 00
0. 175000E 02
0.175000E 02
0.183000E 02
0.185000E 02
0.157000E 02
PERCENT S02
0.0
0.0
0.0 	
0.0
0.0
0.0
0.0
0.0
0.0 	
PERCENT C02
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0,0
MOLAR CONC H2S
0.0
O.IOIOIOE-OI
0»806452E-02
0.212121E 00
0.212121E 00
0.223990E 00
0.226994E 00
0.1862AOE 00
0««28571£ 00
H2S04 LOADING
CMS ACID/GM C
: O.ie^OOOE 00
: 0.102195E 00
0.212486E-01
-0.975879E-01
-0.135261E 00
-0.171670E 00
-0.206<>9<»E 00
-0.2*5341E 00 :i
-0.256918E 00 ;
RATE ACID DECOMP.
GM ACID/GM C-M1N.
0.0
-0.538193E-02
-0.5*1086E-02
-0.251157E-02
-0.251157E-02
-0.234293E-02
-0.230025E-02
: -0.287930E-02
0.563822E-03
  ACID LOADING =    0.184000E-01  AT     0.307191E  02 MINUTES
  RATE_OF_ JVC. ID _DECOMPOS IT I ON. .=	-0.53^137E-02 AT	0. 30 7191E 02 MINUTES
  AVERAGE RATE OF ACID  DECOMPOS'lTION UP TO 90 PERCENT ACIOUTILIZATION =   -0.539510E-02

-------
                           APPENDIX A-16-4

           (NH4)2S EXTRACTION EXPERIMENTAL  RESULTS
RIM:       RXT-T-1C

CARBON USED:  RXT-T-1B
SOLVENT USED:  15?
                  Solution
Waiih Number
1





2



3



b



5



6



' T



6



9



10


i


2


3"


Time,
minutes
0
2
5
8
11
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
>
10
15
0
5
10
15
0
5
10
15
0 •
5
10
15
0
5 -•
10 -
15
0
5
10
0
5
10
0
5
10
Temperature ,
°F
100
102
105
105
105

120
111
110
103
105
102
105
108
110
107
107
105
102
101
102
100
115
ICO
100
103
120
105
105
105
105
107
100
100
110
100
105
100
115
108
105
105
95
100
110
110
105
110
305
105
105
Circulation Rate, ml./mln.
(NHIiJaS
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
91-
->^
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35









H20









































60
60
60
60
60
60
60
60
60
ml. (HE It) 28
Added
~50





-50



~50



—50



-50



-50



^50



,-50



~50



-50











ml. (NHltJj: +
Sulfur Dralr.ed





19-5



36



37



36



3li.5



32



32



32.5



33


30


l46«


37*


39*
      ••1. HjO Dr«in«4
     ••After mtcr vmehlng, Bteamed for 2 hours at 1,000 cc/min.
                                  462

-------
CA'UOIl I '.Ml: R»
Vftcli Kvjalwr
2
3
*
5
6
7
0
9
10
11
12
13
111
15
1
2
3"
T-7-2»
Time,
0
5
10
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
: J
10
15
0
5
10
15
0
5
10
3;
0
5
10
15
0
5
10
15
0
5
10
15
0
10
15
0
5
10
15
0
5
10
15
0
J
10
15
0
5
10
15
0
5
10
15
POLUTIOII arm: i^J (i.',:i,).,:! :;cjutlon
'!''•.', iviiture ,
102
106
105
111
110
100
106
115
109
109
111 .
103
110
10k
109
115
105
105
J09
1X0
)00
110
103
117
100
109
105
120
100
102
123
100
110
98
112
110
105
111
110
110
69
106
110
100
110
102
111
111
112
103
110
110
90
100
112
90
110
110
310
327
105
110
110
120
111
111
111
i'"r ]~'^~ r '^j
35 '
35
35
Vi
35
.35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35


















60
60
60
60
60
60
60
60
60
60
60
60
p.!, (KIU,);;:
—50
-50
-50
-50
-50
-50
-•50
-50
~50
-50
-50
-50
-50
-50
~50



nl . (!i!l|,Nf! *
t'ul f'lf rr:»!no1
25
«2
25


llO
29.6
U6.2
53
51.5
1.2
1.8
1.8
lib
82.5
36.5'
!2.5«
66.3"
"After vater vn
                   it«nm«d for 2 hour* n,t 1,000 cc/mln.
                      463

-------
     RXT-7-3C
CWKSI U1ED: BXT-7-3H SOLVENT USED! 151 (HIH^S Solution
V&Blt Itiunlitr
1
I
3
H
5
6
7
6
9
10
11
12
13
it
15
1
P
f"
Tlr,e,
rtltvit'e
0
5
10
15
0
5
10
15
0
5
ID
15
0
5
10
15
0
5
10
15
0
5
10
15
0
•>
10
15
0
5
10
15
0
•5
in
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
100
15
0
5
10
15
0
5
10
Ttfovcrriture,
•T
105
102
105
105
112
100
106
100
110
100
IOC
10?
102
100
101
101
101
95
101
101
105
100
101
101
101
101
101
101
100
98
101
100
100
101
100
102
101
101
101
100
101
100
101
100
98
100
101
102
105
101
101
100
101
95
102
10?
110
100
lOli
102
103
101
101
101
100
101
101
100
100
105
101
Clrculitlon fljtlt.-, ri)./«.ln.
fuiiii)?;'
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35



KiO















60
60
60
60
60
60
60
60
60
60
60

"''/JuM1*5


50
50
50
50
50
50
50
50
50
50
50
50
50
70"
50«
50-

Sulfur PrnlnM
16
1.5
51
U
1.8
U7
>*
50
VI
37
10
17

55
1,6
111."


  •U. IlpO A t>iuln-d
•"After water vuolilng, ntnuw-il for 2 houra fit 1,000 cc/mln»
                           464

-------
             RXT-T-liC
CARBON
                                BOIVHIT USEDi  15?
                                                         Solution
Vni.li llu«l«T
1
2
3
k
>
6
7
8
9
10
I
11
12
13
111
15
1
2
3"»
Time.
ml mi I* it
0
5
10
15
•K .
•10
»....
: o -
i 5 .0
10 •
W '...
0
5
19
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
Q
5
10
i;
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
J
10
15
Ttimjif ruture ,
Op
100
95
J101
101
105
101
102
102
110
102
103
103
100
103
103
103
110
10?
102
102
lOll
10?
105
105
95
100
100
100
106
100
101
IIS
91
95
1CI>
100
91
99
101
100
108
100
ICE
103
99
105
101
98
90
99
100
100
91
100
100
101
91
100
K'l
103
95
96
100
103
90
106
112
1H
190
126
J25
118
Circulation Fta
.. («!II,)?S
35
35
35
35
35
35
35
35
35
3?
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35



te, nl./nln.
H?n









•





60
60
60
60
60
CO
60
Co
60
£0
ft) '
CO
Bl. (BnO?s
Aisled
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50"
50"
50"'
«ll. (KI!,,S .!•: »
Sulfur I'rH, -1
52
n
i
1.9
1.7
1.9
51
51
1.8 •
U
53.5
S3
55
51
1.8
eo
Ii5«
59"
tg»
            »1. ll?0 Added
            •1. II.-O llrtlnod
            AftKr water wnahlnKi •tpwned  for t houra fti  1(000 cc/lnil).
                                    465

-------
KSl!         MT-1-5C

CARBON UGO>!  RICT-7-5B
SOLVENT VSED:  15* (HH|,)zB Solution
V»h Kumber
1
2
3
14
b
6
7
8
9
10
31
ia
13
lit
15
1
2

Tln.e,
alni!t>>n
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
0
5
10
15
0
5"
10
i;
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
.15
0
5
10
15
0
5
10
15
0
10
15
0
5
10
15
0
5
10
15
Teir.s*ruture,
'f
100
es
90
103
100
100
109
10?
ICO
100
100
100
100
100
100
100
100
100
100
ICO
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
ICO
100
100
100
ICO
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
Cliviil.alon lii
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
as
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35



li-io "















65
«5
65
65
65
65
65
65
65
65
«5
6;
ml. (»i!i.):?s
AdiV>!
100
50
50
50
50
JO
50
50
50
50
50
50
50
50
50
100*
50"
50*
ml. (hMI.)?:'>
Rul fur IH-Rlnpd
1.9
1.6
111
50
59
50
19
60
1.8

1.2
50
1.3
*
50
56"
50"
1.6"
          •nl. ll.iO Added
         •*nl. H.,0 Druliioil
        •«»ft»r untcr vinli
                               utenmed for 2 Hour» »t 1,000 tc/«ln.
                                      466

-------
KUHt          RXT-7-6C

C/UIBOK USKD:  SXT-T-6B
                               SOtVm USEDl  15*
Wash Humtwr

1
2
3
14
5
c
T
8
9
10
11
1?
13
ll>
15
1
i
3...
Time,
mlmiteg
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
15
0
5
JO
15
0
5
10
.ly
0
5
10
15
0
5
10
15
0
5
10
15
0
5
10
35
0
5
10
35
0
5
10
15
0
5
10
15
0
5
10
15
0
»
10
15
T> mpc r ttture ,
°F
100
120
100
100
100
100
100
100
95
100
100
100
100
100
100
105
105
105
105
105
110
105
100
100
95
100
100
100
105
100
100
100
95
100
100
110
95
100
100
100
95
100
100
100
105
100
100
100
105
100
100
100
95
100
100
100
105
100
100
ICO
100
10*,
105
105
105
105
111
110
110
110
..CJrcul.tlnn Rut
dim)-:!
35
35
55
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35
35



e. »l.Mn.
M















60
Co
Co
60
to
£o
60
60
Co
CO
Co
60
nl. (NUl);S

91
50
50
50
50
50
50
50
50
50
50
50
50
50
50
100"
50"
*'
ml. (HI! ) S «

1>5

19
1.6
16
5k
53
fc2
lift

57
H
50
51
k3
72
5P"
75"
  •ml. >l?0 AcMrd
 "ml. lljO Umliied
•"Aftrr vnur m>nlilnr,< lt««m"l fur ? houri
                                                    1,000 cc/Rln.
                                        467

-------
                  APPENDIX A-16-5

PORE VOLUME DISTRIBUTION RUNS FOR  (NH4)2S  EXTRACTED
   AND H2S GENERATION SAMPLES AFTER  SIXTH  CYCLE
                    SAMPLE:  EXV-1
               REL  P
VOLUME
0. 1428
0. 1789
0.2149
0.3251
0.4313
0.5395
0.6477
0.7559
O.C641
0.9722
0.3628
0.3606
0.3733
0.3851
0.3950
0.4031
0.4103
0.41 6.8
0.4242
0.4350
                S    667.4
                C      -22.544
                R  0.9985
           PORE RAUIU!
     VOL
CUMV
1000.
500.
400.
300.
200.
150.
10U.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
13.
16.
14.
12.
10.
0.0022
0.0009
0.0014
0.0024
0.0022-
0.0040
0.0012
0.0015
0.0019
0.0025
0.0034
0.0023
0.002H
0.0035
0.0047
O.OOfO
0.0115
0.0071
0.0096
0.0123
0.0149 '
0.0204
0.0022
0.0031
0.0045
0.0070
0.0092
0.0131
0.0144
0.0159
0.0178
0.0203
0.0237
0.0260
0.0238
0.0323
0.0369
0.0439
0.0554
0.0625
0.0721
0.0044
0.0994
0.1198
                        468

-------
           SAMPLE:  RXT-6-6C
         REL  P
VOLUME
0.1487
0.1863
6.2238
0.3365
0.4492
0.5619
0.6745
0.7872
0.8924
0.9900
S
C
R 0.
0.4417
0.4461
6.4532
0.4688
0.4794
6.4838
0.4922
0.4995-
0.5075
0.5156
794.2
-20.632
9986
PORE RADIUS
VOL
CUMV
1000.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
16.
14.
12.
500.
400.
300.
200.
150.
100.
90.
80.
70.
60.
50.
45.
40.
35.
30.
25.
20.
18.
	 16. 	
14.
12.
10.
„ 0.0006 ..
0.0004
0.0008
0.0017
0.0018
0.0037
0.00i2_
0.0015
0.0020
0.0026
0.0037
0.0024
0.0030
0.0039
0.0059
0.0081
0.0058
0.0043
0.0100
0.0153
0.0215
0.0301
0.0006
0.0010
0.0018
0.0034
0.0053
,- '0.0090
. ._.. 0.01 0.2...
:o.oii7
0..0137
0.0163
0.0199
0.0223
0.0253
0.0292
0.0350
0.0431
0.0489
0.0532
0.0632
0.0785
0.1000
0.1301
             469

-------
          SAMPLE:  RXT-7-6C
         REL P
VOLUME
0.1487
0.1863
0.2238
0.3365
0.4492
0.5619
0.6745
__0.7872
0.8999
0.9900
0.3417
0.3490
0.3530
0.3646
0.3742
0.3823
0.3895
0.3959
0.4031
0.4099
           S    617.8
           C     -20.604 _
           R  0.9983
PORE RADIUS
VOL
CUMV
1000.
500.
400.
_ .300. 	
200.
150.
IOQ*_
90.
80.
	 70. 	
60.
50.
	 45. 	
40.
35.
_ . 30.......
25.
20.
	 18. 	
16.
14.
12.
_ 500.
400.
300.
._200.
150.
100.
	 9.0,
80.
70.
60.
50.
45.
	 .40., 	
35.
30.
	 25.
20.
18.
	 16,
14.
12.
10.
0.0008
0.0004
0.0007
0.0015
0.0016
0.0031
,.Q,OQIO _
0.0013
0.0016
0.0022
0.0031
0.0021
. 	 0,0026..
0.0034
0.0047
0.0070
0.0112
0.0071
— 	 0.0093 _
0.0119
0.0147
0.0185
0.0008
0.0012
0.0020
0.0034
0.0050
0.0081
0,009}
0.0104
Oo0120
0.0142
0.0173
0.0194
__.0.,0220_
0.0254
0.0301
.___0..0371
0.0483
0.0554
, 	 0^0647:
0.0766
0.0914
0.1099
            470

-------
                       APPENDIX A-17
    POST-TREATMENT RESULTS OF AMMONIUM SULFIDE SOLVENT
                     EXTRACTED CARBON
1.   Experimental Conditions for Isothermal and          472
      Thermal Post-Treatments of (NH4)£S Extracted
      Carbon

2.   Experimental Results for Determination of the       475
      S02 Activity of Post-Treated (NH4)2S Extracted
      Carbon Samples Using Differential Rate
      Apparatus

3.   S02 Sorption Rates for Determination of the         486
      S02 Activity of Post-Treated (NH4)2S Extracted
      Carbon Samples Using Differential Rate
      Apparatus
                            471

-------
                               APPENDIX A-17-1

                EXPERIMENTAL CONDITIONS  FOR ISOTHERMAL AND
           THERMAL POST-TREATMENTS  OF  (NH4>28  EXTRACTED CARBON
RUN NO.:

TYPE CARBON:

DESCRIPTION OF RUN:
EXPERIMENTAL CONDITIONS:
RXT-T-6C-1

RXT-7-6C

Run at 1000°F for 2  hrs. with 30% H2

Weight of Carbon:    0.5 gms
Bed Temperature:   1000°F
Inlet H2 Concentration:   30%
Gas Flows:   N2 - 19A cc/min.;    H2 - 8.3 cc/min.
RUN NO.:                 RXT-7-6C-U

TYPE CARBON:              RXT-T-6C

DESCRIPTION OF RUN:       Run at 800°F for U hrs. with H2;  2 hrs . preheat time

EXPERIMENTAL CONDITIONS:  Weight of Carbon:   0.5 gms
                         Bed Temperature:   800°F
                         Inlet -H2 Concentration:   305?
                         Gas Flows:  N2 - 19-U cc/min.;    H2 - 8.3 cc/min.
RUN NO.:

TYPE CARBON:

DESCRIPTION OF RUN:

EXPERIMENTAL CONDITIONS:
RXT-T-6C-5
RXT-7-6C

Run at 1200°F for k  hrs. with H2;  2 hrs. preheat time
Weight of Carbon:    0.5 gms
Bed Temperature:   1200°F
Inlet H2 Concentration:  30%
Gas Flows:   N2 - 19.!+ cc/min.;    H2 - 8.3 cc/min.
                                      472

-------
RUN NO.:                   RXT-7-6C-6

TYPE CARBON:               RXT-7-6C

DESCRIPTION OF RUN:       Run at 1000°F for U hrs. with H2

EXPERIMENTAL CONDITIONS:  Weight of Carbon:  0.5 gms
                          Bed Temperature :   1000°F
                          Inlet H2 Concentration:   30$
                          Gas Flows:   N2 - 19.^ cc/min.;
                                                             H2 - 8.3 cc/min.
RUN NO.:

TYPE CARBON:

DESCRIPTION OF RUN:

EXPERIMENTAL CONDITIONS:
RXT-7-6C-7

RXT-7-6C

Run at 1000°F for U hrs. with N

Weight of Carbon:  0=5 gms
Bed Temperature:  1000°F
Inlet H2 Concentration:  0
Gas Flows:   N2 - 27-7 cc/min.;
                                                             2 hrs. preheat period
                                                             H  - 0
RUN NO.:
TYPE CARBON:

DESCRIPTION OF RUN:
EXPERIMENTAL CONDITIONS:
RXT-7-6C-8
RXT-7-6C
Run at 1000°F for
Weight of Carbon:
                                              hrs. with CO;  2 hrs. preheat period
                                             0.5 gms
                          Bed Temperature:  1000°F
                          Inlet CO Concentration:
                          Gas Flows:   N2 - 19-^ cc/min.;
                                                            CO - 8.3 cc/min.
                                       473

-------
RUN NO.:
TYPE CARBON:
WEIGHT OF CARBON:
DESCRIPTION OF RUN:
RXT-7-6C-9
RXT-T-6C
0.5 gms
(1)  Washed for 15 minutes with 50 ml. of a 2% NH^OH  solution
     at 77°F
(2)  Three distilled H20 washings of 50 ml for 15 minutes
     each at 77°F
(3)  Heat the sample in a 1,000 scc/min. purge of N2  for
     1 hour at UOO°F
RUN NO.:
TYPE CARBON:
WEIGHT OF CARBON:
DESCRIPTION OF RUN:
Virgin Washing with
Virgin, C-70-77
0.5 gms
Same as RXT-7-6C-9
               474

-------
                 APPENDIX A-17-2

EXPERIMENTAL RESULTS FOR DETERMINATION OF THE S02
ACTIVITY OF POST-TREATED (NH4>2S EXTRACTED CARBON
    SAMPLES USING DIFFERENTIAL RATE APPARATUS
                        475

-------
CAICULATIIINS fUK &KAVIHIIHIl flllM l«l'lH|MlNli
MUM NO. •
UMl •
UKV Hl.>
COKRtUION-
Tint
(MINI
1.00
^ 	 2.00
3.00
4.00
5.00
6.00
7.00
6.00
9.00
10.00
11.00
12.00
13.00
14.00
15.00
16.00
1 7. 00
18.00
19.00
20.0(1
21.00
22.00
. . 23.00
24.00
25.00
... . 26.00..
27.00
28.00
29.00
30.00
33.00
	 36.00
, 39.00
42.00
. 	 	 45.00
48.00
51.00
. . .5-4.. 00
57.00
60.00
63.00
66.00
69.00
72.00
' 75.00
78.00
. - ...Bl.OO.
84.00
87.00
.'.^. ..90.00 „
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144.00
150.00
156.00
162.00
168.00
174.00
180.00
IH6.00
142.00
198.00
204.00
210.00
216.00
222.00
22K.OO
2J4.00
240. 00
246. DO
252 . f'U
25H.OO
264.00
270.00
276.00
tH/.PO
2rlil.n(i
244 .5200
0.5200
0.5200
0 5200
0.5200
0.5200
0.5200
0.5200
0.5200
. ......0..5200.
0.5200
0.5200
0.5200
0.5200
0.5200
g.5200
0.5200
0.5200
	 _. 0,5.200.
0.5200
0.5200
0.5290
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5206
0.5200
0.5200
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650'
0.5650
0.5650.
0.5&50
0.5650
0.5650
0.5650
0.5650
.0.565J
0.5650
0.5650
0.5650
0.6050
0.6050
0.6050
O.fcO'-O
0.605D
P.W50
0.6'J^l)
0.6.150
0.6.1MI
O.M'M)
C.fcC'M
O.CPIO
11.KI50
0.<*>>SO
. 	 _ D.6050
O.hOSO
P.C..1SO
0. 6^50
O.M'SO
2000. PPM HUP •
150. PPK Fl 'I "
J.5 < M2iU4 *
6.0 I
CHART
INCHES
7.40
8.0A
8.16
B.27
8.36
8.49
8.60
8.70
8.80
B.91
	 9.0.2...
9.14
9.22
. . . . ... ..9-31 .
9.42
0.52
0.62
0.71
0.81
0.91
1.02
1.14
.25
.36
.47
*58
.69
.79
J.90
2.00
2.32
2.66
2.98
3. JO
j ,63
).9~6 '
4.28
4.60
4.91
5.23
5. 56
5.89
6.21
6.52
6.86
7.19
7.51
7.83
8.16
B.47
8.79
9.10
0.34
0.66
0.97
1.27
1.57
1.87
	 	 2,11 	
2.47
3.05
3.62
4.19
4.77
5.32..
5.88
6.41
. _ .._ 	 6.95 .
/.49
8.00
8.59
0.45
1.41
1.85
2.24
2.72
3.15
4.56
1.97
4.J8
4.77
5.16
5.54
5.42
6.24
6.66
7.0U
1. 11
1. 11}
8.04
2OU. DIG. r.
15CO. CC/MIN 	
75.14 S

PICKUP
IMG H2SO4I
1.61998
. 	 1.75998.
1.87997
1.9N947
2.09996
2.20998
2.3149U
2.4199B
2. 51997
2.62997
Z. 73997
2.B5999
2.93997
3.0299U 	
" 	 3.I399S
3.2.3997
i. 13998
3.42998
3.52998
J. 62997
3.7S9V7
3.80999
3.96999
4.07997
4.U997
	 r 	 4., 2999.1. 	
4.40197
4 ,,5099 8
. 4.61998 	
4.71999
5.03998
	 5,37997 	
5.69998
6.01997
6B3'*990
6. 67990 	
6.99998
7.31998
7.62997
7.94^40
8.27998
0. 60999
8.92998
9.23997
9.57997
9.90997
10.22998
10.54997
10.87997
11.1H997
11.50998
11.81998
12.05998
12.37997
12.68997
12.98997
13.28998
13.5B998
	 	 . J 3. 88998
14.18997
14.76997
. 	 _ 15.3)998
15.90997
16.48997
	 17.03998
17.59998
18.12997
	 _. . 16.66998
14.20908
19.71999
	 20.21494
20.66448
21.12497
2 1.56-148
22.00448
22.41497
22.8649ft
23.27998
21.6H44T
."•4.09498
24.40941
24.67497
25.2549S
2"1 . 6 J44H
20.00146

2I>. 71944
27.0H'I'IU
21.419'iH
2 7. 7*i *'IU
                      476

-------
tALUIlAIIIUll II.K u
                      Ull. rili
RUN NM. »
DA 11 «
DRY WT..
COKREC HUN-
TINE
l.CO
z.oo
3.00
4.00
5.(/0
6.00
7.00
8.00
9.00
10.00
11.00
12.00
13.00
	 	 .14.00 ..
15.00
16.00
17.00
18.00
19.00
.20.00
21.00
22.00
	 J3.00
24.00
2'*. 00
	 	 26.00.-
27.00
28.00
	 ... 27.00 .
30.00
33.00
_.. 	 J6.DO
39.00
42.00
	 45.00
48.00
91.00
.. -SA.OO .
57.00
60.00
63.00
66.00
69.00
72.00
75.00
78.00
SI. 00
84.00
87.00
90.00
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144.00
150.00
156.00
162.00
168.00
174.00
1HO.OO
lUh 00
192.00
1 9ll. 00
204.00
210.00
216.00
222.00
22(1.00
234. PO
240.00
246.00
252.00
2SH.OO
2*4.00
270.00
2 H«. UO
2H2.00
2HH.OO
2V4.1'0
300.00
189 ',11,- .
8 31 U 1411 *
1H.KI, MG , 02 *
-6.22 HG 1120 »
HASS DIM
0.4'JOO
. 	 _ O.'t'JOO
0.4900
'J.1,'100
O.VIOO
0. VJOO
0.5.300
. 0.5300
0.5100
0.5300
_ 	 0.5100
0. 5JOO
0.5300
	 . .. . ...0..5300
D.4300
0.5300
	 0.5300
0.5300
0.5300
	 0,5300
0.5300
0.5300
	 	 0..5300..
0.5300
0.5300
_. 	 0. 5300..
0.5300
0.5300
	 . 3.5300
0.5300
0.5300
	 	 , 	 a, 5300.
0.5300
0.5300
	 	 0.5300.
0.5300
0.5300
0.5300
0.5300
O.'iJOO
0.5300
0.5300
0.5300
0.5300
0.5300
0.5300
0-5300
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5750
0.5900
. 0.5400
0.5900
0. 5900
0.5900
0.5900
0.5900
0.5900
J.4900
0.5900
d . 5900
0 . 5900
0.5VOO
0.4900 .
0. V'OO
J.VIOO
c.vioo
0.5'JOO
C.VIOO
(.'.d^CO
0.6400
0.6400
O.b'.OO
0 . 1.4 0 0
0 .6400
.d.htri)
O.hiPO
0,6400
O.'i'itiJ
i'.6lPt)
2'IOU. I'M* l| HP • 200.
150. IM'H ||!| • 1500.
3.4 T II21IJ4 = 75.55
6.0 X
i it AH r
7.60
	 	 .._ 7.9} 	 : 	
8.18
8.311
H. 56
B.72
0.86
. 1.03 	
1.21
1.37
	 	 1.53
1.69
1.85
?,00
2.17
2.32
2.47
2.6f
2.77
_ 	 -. 	 -2..9.Q 	 .. 	
J.02
3.16
... 	 	 _. 3,20 	 _ .
3.40
3.50
... 	 ._ .3,60 	 i
3.70
3.80
	 _ .. 3i90. 	 „ 	
3.99
4.34
... ._ 	 	 4.65 	 . 	
5.00
5.31
5,61
5.92
6.21
6n51
6.81
7.10
7.39
7.68
7.97
8.25
8.52
8.81
9..09
0.30
0.59
0.87
1.16
1.43
1.71
1.99
2.26
2.54
2.81
3.09
... 3.35 	 	
3.61
1.09
.1.63 	 	
2.17
2.69
3.20
3.71
4.22
4.73
5.21
5.64
6.17
6.66
7.16
.f.64 . ..
11.13
H.61
4.08
9.44
10.00
0.40
O.K3
1.26
l.6t>
2.09
2.49
2.lt9
3.27
3.65
4.U2
4.^0
!)«,. f.
Ct/hIN
I

PICKUP
(KG M2504)
0.51999
0.829 ft
.09999

.4BOOO
.6'J9<*8
.77998
.95000
2.1299V

2.45000
2.60-199
2,76999
2.92000
3.09000
3.23999
	 3.3H998 	 _
3.52998
1.60999
	 3,81999
3,93')99
4.01999
. . .. ,«•.«. 20000
' 4. 3 1999
4.42000
	 A.51S.9S 	
4. (2000
4i71999
	 ...*.ei'J9» 	
4,90999
5.25999
. 	 5,59999. 	
5.92000
6.23000
6,52993
6.84000
7.12999
7,42997
7.7300C
n. 01999
8,31000
8,59999
8.8H998
5,17000
9,43999
9.73000
10., Q099?
10.21999
10.50999
'10.78999
11.07999
11.34999
11.62999
11.90994
12.17999
12.45999
12.73000
13,00999
13.26999
13.52998
14.00999
14.54999
15.09000
15.60999
16.12000
16,62999
17.13998
17.64999
18.12-J94
18.60999
1 9. 09000
19.57999
20.0f999
20,56000
21.04999
21.52998
21. 90998
22.4S999
22.92000
23.31999
23.74-)')B
24.17999
24.59999
24.009*»9
2">.409'»9
5.111000
6. l(l'»99
6.46'»99
|..'M-I'I9
7. .1 1 V9
                477

-------
rc..< I,H/WH'[ i
RUH Nil. • 191
(Mil • 1 2 It .
ORY WT.- 100.56 PC
CURRCCTIUN* -6.43 Ht
HUE
	 (MINI... ...
1.00
2.00
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
11-00 . .
12.00
11.00
.. .. 14.00 ._ . .
15.00
16.00
17.00
18.00
19.00
20.00
21.00
22.00
. 	 .23.00 	 	
24.00
25.00
26. OQ
27.00
26.00
29.00
30.00
33.00
	 	 36.00
39.00
42.00
45.00
46.00
51.00
. . 	 54.0O
57.00
60.00
63.no
66.00
69.00
	 . .72.00 _ 	
75.00
78.00
... 61.00
84.00
87.00
90. on
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144.00
150.00
156.00
162.00
168.00
174.00
180.00
1H6.00
19?. 00
I9H.KO
204.00
210.00
216.00
222.00
228.00
234.00
240.00
24r>.00
252.00
25H. Ou
264.00
270.00
2 II-. DO
2C2.00
2H".00
294.UO
Ji>;».oc
S02 -
•W • .
02
1120 -
MASS DIAL
	
0.5000
0.5000
0.5000
0»5000
0.5000
0.5009
0.5000
... 0.5000
0.5000
0.5000
0.5000
0.5450
0.5450
	 0,J>450
0.5450
0.5450
_ - 0.5450
0.5450
0.5450
-0.5*50
0.5*50
0.5450
	 . .0.5*50
0^5450
0.5450
0.5.45.0
0.5450
U.545CI
0.5450
0.5450
0.5450
	 D.,5.4.50.
0.5450
0.5450
0.5450
0.5450
0.5450
	 0.5450
0.5450
0.5450
0.5450
0.5450
0.5450
0.5450
0.5450
0.5450
0.5450
0.5450
0.5*50
0.5450
0.5450
0,5*50
0.5450
0.5450
0.5450
0.5*50
0,5*50
0.5450
O.f.450
0.5*50
0.5*50
0.5850
0.5850
0.5650
0.5850
0.5850
0.5850
0.5850
0.5H50
0.5850
O.SB',0
0.5950
0.5850
0.58*0
0.5H50
0.5850
rl. '>t'50
0.5150
0.5ll5i.>
0.11)50
0.5H50
U.-nl'il)
O.'.t!50
0.5H>>u
O.V150
U.«,"K>
0, 6/'»0
0.6/50
O.t..".u
O.l.(".»l
2IIOU. PPM UHC «
|5C. VVH .....HII ..'.
}.5 1 M2S04 -
6.0 (
CHAKI
	 	 JNC MIS ..
7.59
7.8)
8.05
8.2*
B. 41
U.58
8.73
8 • (IB
9.01
9.15
9.28
O.J2
0.45
	 .P..57_ . ._
U.-67
0.78
0,81) w_
0.98
1.07
	 1.16...
.25
.35
.44
.52
.61
J.70
.78
.85
.92. 	
2.00"
2.27
. 	 J?,5tt_..._
2.74
2.97
	 3..2J
3.44
3.66
3.87
4.09
4.30
	 	 ?.* I 	
4.72
4,93
5.1*
5.34
5.55
.... ... . 5.75
5.95
6.15
6.35
6.5*
6.73
6.91
7.10
7.29
7.46
7.66
7.8*
8.02
8.20
8.56
0.93
1.30
1.68
2.04
2.40
2.75
3.09
1.42
t.77
4.10
*.*)
4.76
5.07
5. 19
5.72
ft. 05
6.37'
6.69
7.01
7.32
7.61
.94
.24
.••4
.H2
.12
.42
• 11
.99
2ou. tiro. F.
I5UO. CC/MIN
76.20 t

PICKUP
(MC M2S04I 	
0.59999
0.83998
.05998
.24998
.41948
.511991)
.73999
.88998
' 	 2.01999
2.15999
2.2B999
2.329'H
2.45998
	 ^,.57997 	
2.6799U
2.78998
_. 	 2,811997. .. _._
2.98997
3.07997
	 3,16997
3.25990
3. 35997
3.44997
3.52997
3.61996
3.70998
3. 78998
3.85997
	 ._ 3.92998 	
4.00998
'.,27*97
4.50993
4.7*997
*.'J7997
	 	 	 5.21997 . .
5.44997
5.66997
5.87997
6.09998
6.30997
	 	 7.4i997
t. 72997
6.93997
7.1499B
7.34998
7.55997
7.75998
7.95998
8.15997
B, 55997
8.54997
8.73997
8.91997
9.10997
9.29997
9.48997
9.66997
9.84998
1.0.02997
10.20998
10.56998
10.93997
11.30997
11.68997
12.04997
12.40997
12.75998
	 13.09998
13.*2-)9B
13. 77997
14.10997
14.43-197
14.76997
15.07997
15. 39998
15.72997
1»>.OS<>97
Ib. 37997
16.69997
17.01997
17.32'l«)(
I 7.6 V">7
17.9400)

lB.54-197
It). 1)29 >9
19. 12999
I'l. * 2-199
I'l.ll-fit
l'l.9'»9'IM
       478

-------
LALIULMUIUS Illh blUvlHi IHIL MUM Ln-tklM Nl :•
RUN 'III. •
- . llAtt •
UkV hi..
C&mCT IUN.
TIKf
(MINI
1.00
	 2.00.
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
11.00
12.00
13.00
... ._ 14.00.
15.00
16.00
17.00
Id. 00
1 1.»0
20.00
21.00
22.00
	 21.00
24.00
25.00
11,. 00
27.00
28.00
29.00
30.00
' 33.00
	 36.00
39.00
42.00
. . .45.00.
48.00
51.00
	 	 -54.00
57.00
60.00
. . 63.00
66.00
69.00
.._.._ 	 72.00-
75.00
78.00
81.00
84.00
87.00
90.00
93.00
96.00
99.00
102.00
105.00
1011.00
111.00
114.00
1 17.00
1/0.00
1 26 . 00
132.00
1 18.00
144.00
150.00
1 56.00
162.00
168.00
1 K.OO
mo. oo
Iff. 00
192.00
198.00
204.00
210.00
216.00
222.00
2/8.00
234.00
210.00
2li'. 00
2V. 00
25" .00
! 1-4 . (10
2 1(1. 00
2f>.00
/u.'.ou
lan.Oii
2-K..00
iun.no
l'J2 SII2 •
9 3 71 Nil •
100.90 MG 02 *
-6.13 Mb H21) «
MASS UIAL

0.5000
.. 	 	 	 _„. ..o.vjoo
0.5000
0.5900
O.Vi50
0.5450
0.5450
0.5450
0.5450
0.5450
0.5450
0.5400
0.5450
	 0.5450
0.5-.50
0.5450
0.5',5J
0 . 54 50
0.5450
...O.i'.^O
0 . S'.'jO
0.54 SO
_ . 0.5'iVO
0. ?>'i 'jfj
0.5450
.- 	 	 .... 0.5450 .
0.5450
0.5450
	 	 	 .0.5450
0.5450
0-5450
. 	 0.5150.
0.5450
0.5450
. .. 	 	 	 	 0.5450..
0.5900
0.5900
	 .0.5900
0.5900
0.5900
.. 	 .0.5900
0.5400
0.5900
	 0.5900.
0.5900
0.5900
0.59CO
0.5900
0.5400
_O^ 620 fl
0.6/00
0.62(10
0.6.H10
0.6/00
0.6200
0.6200
0.6200
0.6200
0.6200
0.6200
0.6200
0.6200
0.6200
0.6200
0.6200
0.6200
O.e.'OO
o.e^cy
O.<>700
0.6700
0.6/00
0.6700
O.i>700
0.6700
0.6700
0.6/OO
0.6700
0. t> /fiO
O.M'IC
O.e/00
o.<> roo
0.6700
0.0 1'lO
o.i. mu
u. tt/i>D
0.6/UO
0 . ' 1 *«U
o. /1 5r
n./l-'O
O./l'.ll
2000. PI'M II «!• •
150. PPM fill •
3.5 ( H2SIH •
6.0 <
CHAKT
INLHCS
8.29
	 	 _ 	 8,73
9.14
9.52
0.73
1.08
1.39
_. 	 1.69
1.95
2.21
2.46
2.71
2.94
3.16
3.37
3.60
3.60
4.00
4.20
	 4,40. -
4.59
4.76
4.94
5,11
5.29
	 5 ^4__5
5.61
5.79
5.96
6.13
6.66
7.14
7.62
8.10
	 B..5.9... .
0.01
0.50
0.99
1.47
1.92
? - *9
2.83
. 3.29
. .. 	 .. J.91 ._
4.19
4.63
5.Q8
5.51
5.95
0.41
0./7
1.19
1.60
2.00
2.40
2.80
3.2U
3.59
3.98
4.37
5.13
5.U9
6.60
7. JO
7.99
8.67
9.34
. . 9.V9
0.-.7
1.10
1 .t>9
2.26
2.H/
3.39
3.91
4.44
4.95
•>,44
5.'>
-------
CAICUIAIIONS FlIX ORAVIMlIRIC tLdtl LKPlklMI MlS
BUN NO. * 193
UAU . 9 t 71
DRV WT.- 102. 02 MC
CMKtCMON- -6.18 HG
Tine
	 (UNI ...
1. 00
2.00 	
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
11.00 	
12.00
n.oo
	 14.00
15.00
16.00
17.00 	
18.00
19.00
20.00 . . ._ 	 	
/1. 00
2?. 00
	 23.00
24.00
25.00
	 26.00.
27.00
28.00
	 .29.00 	 „.. 	
30.00
33.00
36.00
39.00
42.00
45.00
48.00
51.00
	 5.4.00. . ..
57.00
to. oo
63.00
66.00
69.00
72.00
75.00
78.00
81.00 	
84.00
87.00
90.0"
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144.00
150.00
15t..t)0
162.00
I Ml. 00
174.00
180.00
186.00
142.00
148.00
204.00
210. 00
2|h.OO
222.00
/28.00
2 14.00
24U. UO
24/i. 110
25/.00
25M.IIU
.'(.4.00
27U.UO
2/h.OU
2H/.DO
/HH.I10
.' '14 . HO
inn. oo
i02 •
'10 •
02 •
H20 •
MASS DIAL

0.5100
-0,51PO_
0.5100
0.5100
0.5100
0.5100
0.5100
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
.0.5550
0.5550
0.5550
. -0^5550
0.5550
O.CtiO
.. 0.5550.
0.5530
0.5550
...0,5550.
0.5550
0.5550
. 0.5i50
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0%. 5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.555G
0.6000
...0.6000
0.6000
0.6000
.0.6000
O.cOOO
0.6000
0.6000
0.6000
0.6000
0.6000
0.6000
0.6000
0.6000
0.6000
0.6000
0.6000
0.6350
0.6350
0.6350
0.6»50
0.6150
0.6150
0.6350
0.6)50
O.l.JSC
0.6 150
0.6350
0.6J50
U.M50
' O.MSO
' O.MSU
" O.dt'iO
' O.MVI
' O.bM'C
o. «.tmj
0.6HOO
U.bl'OO
0. Ml 00
O.l.M'O
J.I.!' JO
O.hHIH)
I). Ml I'D
O.I HIM)
O.MM'lt
2000. PPM TI.KP «
150. PPM F(l| •
3.5 Z H2Sl'4 *
6.0 t
CHART
... . __ 	 IHCHtS
7.63
7, B't
""8.16""
8.40
8.65
tt.to
9.13
0.27
0.49
0.70
0.91
.11
.30
.45
.67"
.Hi
2,00
2.17
2.34
	 	 2,4.9 _.
2.64
2.80
... ._ .2.94 	
3.09
3.22
3..3J
3.5I~
3.63
3..77__
3.90
4.30
4.68
5.05
.41
• 79
.17
.52
,E9
7.26
7.61
7*58
8.32
8.68
9.P2.
9.36
0.87
I * 2.2.
1.59
1 .94
2.30
2.66
3.00
3.36
3.70
4.04
4.37
4,70
5.02
5.34
5.66
6.29
6.91
0.44
1.02
1.60
' 2.16
2.71
...... ' 3.26
3.80
4. 35
4.89
5.. 41
5.41
' 6.44
(..46
7.45
7.44
H.V2
H.90
0.3H
0.82
1 .26
1.70
2.12
1. -.5
Z.'J'j
3.3H
1. 74
4.14
4.5H
200. DEC. ).
15UO. CC/M|^
76.19 t

PICKUP
IMG H2SD4I
0.62997
O.B8998
1.15447
1.39998
1.649VB
1 ,89998
2. 12947
2.26997
2 . 4 (1 9 4 7
2.69998
2.90997
3.10997
3. 29497
	 	 3.40997 	 _
3.66448
3.82997
3.9999B
4. 169VU
4.33998
_ 	 ^__ 	 4.40997 	 	
4.639'JB
4. 79997
4.93447
5.08998
5.21997
_ 	 	 J>i3'»998 	
" 5.50998
5.62997
.._ 	 : 	 _._ 5,76997 	 	
5.89998
6,29997
b. 67996
7.04997
7.40947
7.7899U
8.16998
8.51997
8,8899(1
9,25t.'9B
9.60')97
9.97998
10.31996
10,67998
^ 	 	 	 .._ll,01997 	
11.37997
J 1.86998
12* 21997
12.58998 	
12.93997
13. 29497
13.65997
13.99998
14.35997
14.69998
15.03998
15.36998
15.69998
r 16.01997
..I- . 16.33998
16.65997
17.28998
17.90997
18.43997
19.01997
19.59998
?0. 15997
20.70498
21.25998
21.79997
22.34093
22.88948
23.4094J
23.92448
24.43497
24.9S94B
25.44496
25. 'M49 7
."•6.414'IU
2(i.H444l)
27.37997
2 /. 01 9'ia
21* . 2'»49tt
28.64448
29.| 1498
29. 54497
24.94998
30.37447
3C.7H44H
3t.KI44f
tl. 57491
               480

-------
CAICUIA!IDNi H>K GKAVlMUKIt I I im [(PtHIKtntS
RUN NO. •
DATt -
UK* *l."
CCMRFCIION-
Tlflt
	 IMIN)
1.00
	 2.00..
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
11.00
12.00
13.00
. 14.00
15.00
16.00
.. . 17.00
18.00
19.00
	 20.00 .
21.00
22.00
. . _ . 23.00
24.00
25.00
	 ..26.00
27.00
28.00
_ 29.00
30.00
31.00
.. 36,00
39.00
< 42.00
45.00
44.00
51.00
14 > 00
57.00
60.00
61.00
66.00
69.00
72.00
15.00
78.00
81.00
84.00
87.00
90.00
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00 •
126.00
132.00
U8.00
144.00
150.00
156.00
162.00
168.00
174.00
180.00
186.00
197.00
198.00
204.00
210.00
216.00
727.00
228.00
2)4.00
740. (10
740.00
257.00
258.1)0
264.00
770.00
210.00
787.00
7UH.OO
7-14.00
300.011
194 SO/ * 2000.
9 1 71 NO > ISO.
103.30 MG 02 » 3.5
-5.98 MG M2O • 6.0
MASS DIM

0.5150
.. ... __ . . Q,5150
0.5150
0.5150
O.M50
0.5150
0.5150
0.5150
0.5150
0.5150
	 0.5I5C,
0.5150
0.5150
0.5150
0.5150
0.5600
	 . .0.5600
0-5600
0.5600
	 	 	 0,5600 ... ..
0.->600
0.5600
	 0.5600 	
0.5600
0.5600
0,5600
0.5600
0.5600
0,5600
0.5600
0.5600
. .... ... 0,5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5500
0.5600
0* S6CG
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0.5600
0. 5600
0.5600
U.560U
0.5600
0.5600
0.5600
0.5600
O.SeOO
0.5600
0.560J
0.5600
0.5900
0. 5WO
0.5900
0.5)00
0.5900
0.!>->00
0.5900
U.590J
0.5^00
0.5900
0.5900
11.5900
O.VIOO
0.5"tlO
O.VIOQ
0. V'OO
O.VOO
o.'> too
3,'i'XIO
O.ViOO
O.'.'IOO
O.yiOO
U.V100
U.V100
0. ••">('
U.4'100
Pl'« tlW • 20U.
PPM HI) • 11(10.
< H2SU4 * 75.6V
*
CHART
IMCMFS
/.78
7.87
7.9t
8.06
. 8.16
(1.26
8.37
8.47
8.5*
8.67
B.74
8.82
8.90
8.99
	 9.06"
0.12
.,0.20 	
0.29
0.37
_. .0,45.
0.53
0.61
	 .0.69
0.7£.
0.83
0.8.9
0.96
1.01
.09
.15
.32
. .50
.66
.65
2.01 _
2.18
2.34
2.50
2.67
2.62
2.96
3.10
3.25 '
3.39
3.53
3.67
3. 80
3.94
4.08
4,21
4.34
4.47
4.59
4.12
4.87
5.00 .
5.14
S.27
5.40 . 	
5.54
5.8C
6.0!. . .
6.30
6.55
O.R2
1.09
1.35
1.60 .
l.t>5
7. ID
2.36
2.61
2.86
.3.10
3.34
*.->r
l.HO
4.C7
4.24
4.45
4.65
4.1)5
5.04
5. .'4
'» . 4 It
-J.fc'l
*>.9C
I..I 1
6. Ik
1. .Ml
UL(». F.
Lt/MIN


PICKUP
(MG H2S04)
.49998
.58998
.67998
.77998
.87997
.97998
i 2.08998
2.18997
2.29997
2.38998
2.45998
2.53998
2.61998
2.70998
2.79997
2.83998
	 2.9199H
1.0099U
3.0S19B
3.16*98
3.24998
3.32997
3.40997
3.47998
3.54997
1.6099J}
3.67998
3.72998
3.8099U
3.86998
4.03998
_ 4_. 21999
4.39998
4.56998
4.72998
4.89996
5.05998
5.21999
5.38998
5.53796
5.67998
5.81998
5.96999
6. 10999
6.24998
6.38998
	 6.51997_._
6.65997
6.79997
6.9J998. _
7.05998
7.18997
7.30998
7.43997
7.58998
7.71999
7.85999
7.9B99T
». 11998
B.2599H
8.51997
8.7699?
9.01997
9.26997
9.53998
9.8099B
10.06998
10.31998
10.56998
1C.B19)U
1 1 .07^97
11.32997
11.57997
11.81998
12.059VU
12.289'I8
12.51997
17.73997
17.959'»B
1.1. 16998
11. 164'IU
I.I.56')'Hi
14.40'M/
I4.61'l')tl
I4.lt4'l'll(
1 '< . 0 7 't 't /
ls.,-'rr»i
                   481

-------
C»tCUL»riONl  FIIK GHAvmiKIt  FlUw
RUN HO. •
UAH •
(IKT »!.•
CORRECT KiM-
HUE
(HI'll
1.00
2.00
J.OO
4.00
5.00
6.0(1
7.00
8.00
9.00
10.00
11.00
12.00
13.00
14.00
15.00
16.00
17,00
18.00
19.00
20.00
21.00
22.00
.. 23.00
24.00
25.00
26.00.
27.00
28.00
29.00
30.00
33.00
36.00
39.00
42.00
.. 45.00
48.00
51.00
_...54...00
57.00
60.00
63.00
66.00
69.00
.._ 72.00
75.00
78.00
ai.oo
84.00
87.00
90.0k
93. CO
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
132.00
138.00
144. PO
190.00
156.00
162.00
168.00
174.00
180. PO
180.00
192. PC
198.00
204.00
210.00
216.00
22. '.00
22H.OO
234. PO
240. PO
246.00
252.00
2V..PO
264.00
270.00
27o.l'0
2H.'.OJ
2HH.HP
,"i4 . ro
ll/l'.OO
195 SU2 • 2000. PCM
•1 10 71 (in • l',0. PPK
104.70 HG U2 • 3.5 1
-5.87 MO H20 « 6.0 (
MASS DIAL
.
0.5200
0.5200
0.5/00
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5200
0.5205
c.5200
0.5200
. 0.5650 ..
0.5650
0.5650
0,5650
0.5650
0.5650
. 	 0.5650. 	 	
0.5650
0.5650
0.5650
C.5600
0.5650
. . 0,5650
0.5650
0.5650
, 	 	 	 0.565D _ 	
0.5650
0.5650
jO. 5650
0.5650
0.5650
.. 0,5650. . 	 .
0.5650
0.5650
	 0.5650 	
0.5650
0.5650
0.5650
0.5650
0.5650
	 0.5650 	
0.5650
0.5650
0^5650
0.5650
0.5650
O.'ih'iO
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650
0.5650
0.565P
0.5650
0.5650
0.6100
0.6100
0.6100
O.blOO
0.6100
0.6100
0.6100
0.6210
0.6250
0.62SO
0.6250
0.6250
0. 62V
0.(i25P
0.6250
O.h/SO
0. h2')t1
0.6.">0
0.1.250
<).02'.i>
o.*»2-)0
0.6/'>e
0. t>2'>0
il.(,.".0
O.h2'»0
ll.l/Sl)
O.f. 2'tO
II. (•.">('
U.I.,' '.0
I EMP '
Mil -
M2SU4 •

CHART
IMCMFS
7.49
7.69
7.88
8.04
8.20
«. 35
8.50
8.63
8.76
8.b9
9.01
9.12
9.23
....0.2'. .
0.35
0.46
0.56 .
0.66
0.76
	 .0.87.
0.97
1.06
-1.14
1.24
1.34
1.43
1.51
1.59
i.«.69._.
1.78
2.04
	 4,29,
2.54
2.79
3,04
3.29
i.53
JU 78
4.0l"
4.25
4.49
4.72
4.96
5.19
5.43
5.66
5.9.0
6.13
6.36
6 so
a. 82
7. Ob
7.30
7.54
7.77
8.00
8.23
8.46
S.69
3.91
4.36
C.tll
1.27
1.7)
2.18
2.62
3.06
. I.4B
0.40
l.il
1. /O
2. I'l
.' . t.O
I.UI
1.44
I.H6
• . / '1
4. 10
*•.! 1
•••••I
'..'11
^. 1U
t. . l> -1
i.PI
1.44
7 »ll 2
t . 1 li
C.1)*
I'.ni
'i . .' 3
• 200. ore. F.
1M.O. CC/MIN
76.92 I

PICKUP
(Mb H2SII4I
0.91997
1.11996
1.30447
1.46947
1.62997
1. 77947
1.4249S
2.05997
2.18947
2.3194*
2.43497
2.54497
2.65997
2.66497.
2. 77997
2.88997
2, 989') 1
3.08997
3. 18997
3.29997
3.34496
3.48997
3.56948
3.66-197
3.76997
	 	 , 	 .3. 5)5947. 	 . .
3.43997
4.01997
	 . ...4 ,11 9-9 6 	
4.20998
4.46997
4.71997
4.9690.7
5.21997
5.46997
5.71997
5.95998
	 	 ...... 6, 2099B... __
6.43997
6.67998
6.91997
7.14996
7.38997
7,61996
7.85997
8.06997
8.32997
t. 55997
8.78996
9.01997
4.24997
9.50996
9.72997
4.46447
10.19997
10.42998
. ' 10.65997
10.88997
11.11996
11.33947
11.78996
12.23997
12.69997
13. 15997
U.60'197
14.04'I9;
ll.4H')9(
14.9099/
1 '< . 3/'l94
15. 759-IB
lo. IB'l I'l
16.619 IB
1 7.079'IB
If. 4 »•>•(•»
17. Hf.'llIH
If .2H44H
If. /1'1'W
14. 1,"|.| 1
I'l .5 I'HH
l'l.9 ).|'I4
2f. ll'l'ld
20. /24'lrt
21. 1 1'1'IH
21. 4'lrl'IB
21.H(,'M,1
22. '4'l9il
/,' 
-------
IALCUIAI IDNS ru« GKAVIMHRIC HUW
HUN NO. • 196 502 • 2000. PPM
DATE • 9 14 71 (W » lr>q. PPH
DRY HI.- 100.42 HC O2 • 3.5 »l
COKRECtlON' -6.22 MO H20 • 6.0 I
TIME
. .IMINI
i.oo
	 ..2.00.. 	
3.00
4.00
...5,00
6.00
7.00
8.00 _
9.00
10.00
. . 11.00 . . .
12.00
13.00
._.14.00 	
15.00
16.00
. . _..17.00 	
18.00
19.00
	 20.00 	
21.00
22.00
.. _ 23.00 	
24.00
25.00
_ ..26.00 	
27.00
28.00
29.00
30.00
33.'00
36.00
39.00
42.00
4 5.. 00
48.00
51.00
54.00
57.00
00.00
	 63. .00 .. _
66.00
69.00
17.00
75.00
78.00
81.00
84.00
87.00
90. nn
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
120.00
126.00
132.00 . .
1 Jfl.OO
144.00
150.00
156.00
162.00
168.00 	
174.00
IbO.OO
186.00
192.00
198.00
204.00
210.00
216.00
222.00
228.00 •
234.00
240.00 	
246.00
2*2.00
264.00
270.00
? IA nn
2B2.00
288.00
294.00 	
300.00
MASS DIAL
0.5000
	 O.SOOO
0.5000
0.5000
	 ,0.5000..._
0.5000
0.5000
.. . 	 0.5000
0.5000
0.5000
. 	 . 0.5000
0.5000
0.5000
..... ... . _0,5000 . .
0.5000
0.5000
	 	 	 	 0.5.00D
0.5000
0.5000
	 0.5000
0.5000
0.5000
. 	 0.5000
0.5000
0.5000
p. 5000
0.5000
0.5000
	 o.r,ooo
0.5000
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5-400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400 .
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.5400
	 	 9,5400.. 	
0.5400
0.5400
0,5400
0.5400
0.5400
0.5400
0.5400
0.5400
0.540Q
0.5400
0.5400
0.6400
0.5400
0.5400
0.5400 	 _ ...
0.5400
0.5400
_ 0.5400 	 _ ...
0.5400
0.5400
0.5400
0.5400
0.5400
0.540D
0.5400
0.5400
0.5.400 . _
0.5400
0.5400
0*5400
0.5400
n»f > 200. ore,. F.
f 1 [| • 1500. CQ/MIN
t«S04 • 75.78 I
CHART 1
HIGHER (M!
7
7
7
7
7
7
7
f
7
7
a
8
8
8
8
8
8
8
8
8
8
8
8
8
8
a
8
8
8
8
0
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
.44 (
.54 (
.60 !
.65
.71
.77
.82
.88
.93
.98
.04
.10
.16
,2_1. 	 	 	 	
.26
.31
.36
.40
.44
• 19
.54
.59
.63
MCKUP
;_ii2S04) 	
). 79999
1.89999
). 95999
.00999
.06999
.12999
.17999
.23999
.28999
.34000
.39999
.45999
.51999
.56999
.62000
.67000
.71999 ___
.75999
.79999
.84999
.89999
.95000
.98999
.68 2.03999
.72 2.07999
.76 2.120DO
.so ;
.85 i
'.•}} ";
.93 i
,0.3 	 <
.14 i
.26 i
.37 i
.48 ;
.59 i
.6? 3
.79 :
.69 :
'!'09 3
.19 :
.29 5
'.15999
'.20999
'.25000 	 .
'.28999
'.28998
'.38998
.49998
.61998
.72998
'.83998
'.94993
1.04997
1.14998"
.3499B
1.44998
1.54997
.64998
.39 3.74998
.49 3.84998
.59 3.94998
2.69 4.04997
2.78 4.13998
2
3
3
3
3
3
3
3
	 3
3
3
4
4
4
4
4
4
5
5
5
5
5
6
. 6
6
J»
6
6
7
7
7
7
.7
7
8
,.. 8
a
8
. 8
.97 4.32997
.06 4.41998
.15 4.50998
.24 4.59998
.32 4.67998
.40 4.75998
.49 4.84998
.57 4.92998
.66 5.01997
.74™ 	 	 " 5.09990
.90 5.25998
,08 . . 5.43997
.26 5.61998
.44 5.79997
.61 5.96997
.80 6.15997
.98 6.33998
,16 , 6;51997
.34 6.69998
.51 6.86998
.70 7.05998
.87 7.22998
.05 7.40997
.72 7.57997
.40 7.75998
.58 7.93997
.75 8.10999
.93 	 ~ 8.28998
.10 8.45998
.27 ....... 	 ..8.62997 	
.43 8.789V8
.60 8.95998
-77 9.12997
.94 9.29997
.10 9.45998
.27 9.62997
.44 9.79997
.60 9.95998
.77 10.12997
B.91 10.28998
                       483

-------
CALCULATIONS FUR  GKAVIMUHIC  HI,.! CXI'CHlMbNTS
RUN NO. •
DMt •
DRV Hi.-
COHRfCT ION"
TIME
I«!NI
1.00
2.00
3.00
4.00
5.00
6.00
7.00
. 8.00 	
9.00
10.00
1KOO
12.00
13.00
14.00 .
15.00
16.00
17.00
18.00
19.00
20.00
21.00
22.00
23.00
24.00
25.00
	 __26.00_. .
27.00
28.00
29.00
30.00
33.00
36.00
39.00
42.00
45.00
48.00
51.00
S4.00
57.00
60.00
63. 00
66.00
69.00
J2.0.0 _
, 75.00
78.00
fll.nn
84.00
87,00
on. on
93.00
96.00
99.00
102.00
105.00
100.00
111.00
114.00
117.00
120.00
126.00
132.00 .
\iU.UO
144.00
_. 150.00
I5(..<>0
162.00
168.00
174.00
180.00
106.00
192.00
198.00
204.00
210.00
216.00
222.00
228.00
234.00
240.00
246.00
757.00
„ 	 2b.a.co..
264.00
270.00
216.00 .
282.00
200-00
294.00
300.00
197 S02 • 2000. PPM
9 15 71 _ HI) » j 50. PP«
Vfl.30 MC 02 • "" 3.5 X
-6.09 MC H20 • 6.0 »
MASS DIAL
0.4900
0.4900
0.4900
0.4900
0. 4VOO
0.4900
0.4900
.. 	 0,4900 	 . 	
0.4<)00
0.4900
0.4900
0.4900
0.4900
0.4900
0.4'!00
> 0.4900
	 O.',900
0.4900
0.4900
0.4900
0.4900
0.4900
	 0-4-(00 	
0.4900
0.4900
	 0.. 4.90.0 	 	
0.4900
0.4900
0.4900
0.4900
0.5350
0.5J50
0.5300
0.5350
0.5350
0.5?50
0.5350
0.5*50
0.5350
0.5353
0.5300
0.5350
0.5350
0.5350 , ,
0.5350
0.5350
0.5350
0.5350
0.5)50
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
. . . 0.5359 _
0.5350
0.5350
	 0.5}',0 _.„ .
0.5350
0.5350
0.5350
0.5350
0.5350
_0.535Q
0.5350
0.5350
0,5350
0.5350
0.5350
0.5)50
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5350
0.5J50
O.S1SO
O.SJSO
IfHf • 200
FID « ...151.0.
112 SO* " /4.73
CHART
INCHC-S
7.52
7.63
7.70
7.77
7.83
7.89
7.96
_...8,P2 	
8.09
8.15
8.21
8.28
8.34
8.40
8.45
8.50
8.54
8.59
8.64
8,69
8.74
8.78
8.8? .
8.116
8.90
..J1..94 	
B.9B
9.02
9.07
9.11
0.08
0.19
0.30
0.41
0.52
0.62
0.73
0.83
0.93
!.04
1.1 'i
1.25
1.36
1.47
1.57
1.67
1.77
'..86
1.96
2.06
2.15
2.25
2.35
2.45
2.55
2.65
2.74
2.84
7.93
3.01
3.20
_.- ».»«.. _ .._
3.57
3.75
,.3.93. 	
4. 10
4.30
4_,48
4.65
4.02
5.00
5.18
5.35
5.52
5.70
5.88
6.06
6.24
6.42
6.60
6. BO
6.98
'•*•*,
7.35
7. S3
7.70
7.89
8.07
6.23
8.39
. OEG. F.
CC/MIN 	
I
PICKUP
(Hb H2SU4I
1.12997
J.2399.7_ _
1.30998
1.37997
1.43997
1.49998
1.56998
1.62997
1.6999!)'
1.75998
1.B1998
1.88998
1.94998
2.00998
2.05998
2.10999
2. 14998
2. 19990
2.24998
2.29997
2.34998
2.30998
2.42998
2.46997
2.5099B
2.54997 	
2.58998
2.62997
2.67998
2.71997
2.68997
2.79997
2.90997
3.01997
3.12997
3.22998
3.33998
3.43997
3.5399B
3.64998
3.7*998
3.85999
3.96997
4.07997
4.17998
4.27998
4.37997
4.46997
4.56998
4.66998
4.75996
4.85999
4.95998
5.05998
5.15997
5.25998
5.34998
5.44998
5.53998
5.61998
5.80998
5.99998
6.17998
6.35999
6.53998
6.70998
t. 90997
7.08998
7.25998
7.42998
7.60999
7.78998
7.95998
8.1299T
8.30998
8.48997
8.66998
8.84948
9.02998
9.20998
9.40997
«. 56998
9.77998
9.95998
10.13998
10.30998
10.49998
10.67998
10.83978
10.99998
                       484

-------
CM.CULA1ION& F(lK GRAVIMETRIC FIOH
P.IIN NO. > 198
UAIC •_ .9 Ib
DRV WT." 103.10
CORRECTION* -5.10
...

—
—
-

-
TIME
(MINI
1.00
._ 2.00 	 _
3.00
4.00
5.00
6.00
7.00
8.00 	
9.00
10.00
	 11.00
12.00
13.00
..14.00 _ 	 „
15.00
16.00
	 17.00 	
18.00
19.00
.. 20,00.. .. ... _
21.00
22.00
. 23.00 _
24.00
25.00
. 26.00 	 	
27.00
28.00
29..00
30.00
33.00
	 36.00 	 	
39.00
42.00
45.00
48.00
51.00
54.00
57.00
60.00
	 63.00 	
66.00
69.00
7J.OO
. 75.00
78.00
ni.no
84.00
87.00
90.00
93.00
96.00
99.00
102.00
105.00
108.00
111.00
114.00
117.00
120.00
126.00
J32.00
138.00
144.00
150.00
156.00
162.00
Ib8.00
174.00
180.00
la(>, oo
192.00
198.00
204.00 	 	
210.00
71b.OO
222.00
228.00
734.00
24,0.00
246.00
25?. 00
256*00
204.00
270.00
27b»00
782.00
2 1)1). 00
294 .00
300.00
SII2 • 2000. PPM
71 HO « (50. PPM
KG 02 • 3.% *
MB H2U ' 6.0 *
MASS DIAL
0.5100
0.5100
0.5100
0.5100
0.5100
0.5100
0.5100
J>.5100 ..
0.5100
0.5100
0.5100
0.5100
0.5100
	 0, 55.50 	 . 	
0.5550
0.5550
.. . __..0, 5550
0.5550
0.5550
0.55SO
0.5550
0.5550
	 	 .0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
O.SI'.O
0.5550
0.5550
0.55'jO
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5050
	 0.5550 _ 	 	 	
0.5550
0.5550
0.5550
0.5550
0.5550
O.5550
0.5550
0.5550
O.S550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.5550
0.4550
0.5550
0.5550
0.5550
0.5550 	
0.5550
0.6000
0-6000
O.bOOO
0.6000
O.bOOO
0.6000
0.6000
0.6000
O.bOOO
0.6000
O.hOOO
0.6000
0.6000
0.6000
0.6000
0.6000
p.6000
0.6000
0.6000
0. 61)00
O.hOOO
0.6400
0.6400
T6MP .
Fit) •
H2SD4 >
CHART
INCHES
8.11
8.19
8.27
8.34
8.42
8.50
8.58
8.67
8.74
8.81
ft. 89
8.98
9.06
0.07
0.13
0.19
9,21
0.34
0.41
0.46
0.55
0.62
0.69
0.76
0.82
O.flS
0.97
1.03
J.JQ
1.08
1.37
-L.57
1.76
1.95
2.14
2.32
2.51
2.70
2.89
3.08
	 3,27._
3.46
3 '.64
. — 3.82
4.01
4.20
4,40
4.59
4.79
4.99
5.18
5.38
5.58
5.77
5.97
6.18
6.39
6.69
6.80
7.01
7.47
7.84
8.25
8.67
9.06
9.49
0.89
-J.2,9
l.bB
2.08
2.48
2.89
3.30
	 J.71
4.11
4. SI
_ .t'1*'
5.36
5.74
*.U
6.S7
6.41
	 1, it
7.69
B.07
	 a. 45 _
8.8)
0.94
	 l.iO_.
1.46
200. UCC. f.
1500. CC/KIN
77.32 %
PICKUP
IMG H2S04I
1.90997
1.9B997
2.06998
2.13998
2.21999
2.29999
2.37997
2.46999
2.51998
2.60999
2.68999
2.77998
2.85999
2.86906
2.92998
2.98997
3.06998
3.13998
3.20998
3.27998
3.34998
3.41998
3.48997
3.55998
3.61998
3.68999
3.76997
3.82999
3.89998
3.87997
4.16998
4.36998
4.55998
4.74998
4.93999
5.11998
5.30998
5.49998
5.68999
•5.R7997
6.06998
6.25998
6. 43999
6.61998
6.80998
6.99998
7. 19998
7.38998
7.58998
7.7B998
7.979V8
6.17998
B. 37997
8.56998
8.76997
8.97998
9.18999
9.48997
9.59998
9.80998
10.21999
10.63998
11.04999
11.46999
11.87997
12.28998 ""
12.68999
13.08998
13.47998
13.87997
14.27998
14.68999
15.09998
15.50998
15.90997
16. 10998
16.74998
17.15997
17.53998
17.9299B
I8.3199U
18.70998
19.00998
I9.4H997
19.8699*
20.24998
20.62997
20.73997
' 20.99
-------
                 APPENDIX A-17-3

 S02 SORPTION RATES FOR DETERMINATION OF THE S02
ACTIVITY OF POST-TREATED (NH4>2S EXTRACTED CARBON
   SAMPLES USING DIFFERENTIAL RATE APPARATUS
                       486

-------
          CAICUIATIONS fllh GkAVIHtlHIL film




     C-70-77 (VIRGIN)




.. .RUN NO, •  180 	
IMH « 9 "»
tut m.. 95.10
.COSKElUllN' -6.18
. MEAN LUAU 	
CMS S02/100 GKS C
0.87202 ...
0.4)410
0.99B43
1.05519
1.11195
1.16871
1.22189
1.27449
1.32867
1.38543
1.44477
1.49637
	 1.54023.: 	
1.59105
1.64601
	 1.69761
1.74663
I. 79565
.. 	 ...1.84725 . .
1.90142
1.96076
	 	 2. U2011. -
2.07686
2.13»M
.- 	 2.19030 .._.
2.24714
2.30132
2.35550
2.40968
2.51604
	 	 	 2.68831 	
, 2.85859
3.02371
3.19141
3.36168
3.52939
.. .3.69450 	
3.B5704
4.01958
4.18728
• 4.35756
4.52525
4.6B779
' 4.B5549
5. 02834
. 1 . 5.19604 . _
5.36116
5.52886
._ 5.69398 ..
5.05651
6.01905
6.16095
6.30543
6.46797
6.62534
6.78014
6.93494
7.0H974
7.24454
7.47157
7.76827
8.06239
6. 15908
8.65062
t. 93700
.9.211)21
9.4')427
9.77291
10.04331
10. 30431
10.54040
10. /K426
11.01645
11.24149
11.467'It
1 I.6H9H2
11.906S4
12.111110
12. 3/91,5
11. •> 16U5
I2.7I//9
I?.')!1)'!'.
1 1.1 I/UI
I3.3/5M
I J.MI.H4
1 \.i:'llr./
1 1. MH.'HO
|4.0' )'. i
14.,' I'*.1',
71 NO • 150.
Cf. 02 « 3.5
MC. . .IliD." 	 6.0.
	 D1FFMENUAL RATE
HOM S02/GM C-M1N
. _ 	 	 0.72239 .
0.61917
0.56760
0.56760
0.56760
0.56760
. .0.516O2
0.51595
0.56760
	 0.56760
0.61925
0.41273
	 	 0.46445 	
0.56760
0.51595
	 	 0.51602 ..
0.46438
0.51602
. 	 0.5159i_,
0.56760
0.61925
	 	 0..56760 	
0,56752
0.56760
..- 	 _ 0.56760 .
0.56760
0.51602
	 0.56760 . ..
0.51602
0.55038
_ 	 	 0.584J9. 	
0.55041
0.55038
0.56760
0.56760
0.55041
0.55036
0.53319
0.55U41
0.56760
0.56760
0.55038
0.53319
0.58479
0.56760
.. ...... 0.55041
0.55038
0.56760
0. 53119
0.55041
0.53319
0.41280
0.5503B
0.53319
0.51600
0.51600
0.51600
0.51600
0.51597
0.49Bt>0
0.49020
0.49019
0.49B60
0.47300
0.4B159
0.45579
0.46440
0.46439
0.43U60
0.429V9
0.3U699
0. »95'>9
0.37H40
O.I7U40
0. I6-JM
0. I6^H()
0. «'-260
0.3'i2'j'l
0.)'>2I>0
0. 13540
O.llViU
0. l^itllO
0. I26HU
O.llHl'
O.Jlal-
U.."'/41
o . 1 1 n r
O.»'r ini
0.? l.'l>
?fn F(T1 • 1SOO.
t H2UI4 * 75.14
-' 	 - 	
MEAN LOAD
CMS ACID/100 &MS I
l.J35?B '
1.4)799
I. 52885
1.61577
1.70260
1. 71)959
1.87256
1.V5157
2.03452
. ... 2.12144 ._._
2.21231
2.29132
	 . _. ..2.J5B4T 	
2.4374'V
2.52045
	 2.59946 	
2.67452
2.74959
2.82860.
2.91155
3.00242
. 	 ..3.0?329_. _
3.1B020
3.26710
.. . 	 Jj 35402 	 _
3.44093
3.52369
3,60666
3.63982
3.B5575
	 	 4,11640. 	 	
4.3T722
4.63006
4.04684
5.14758
5.40437
5.65721
5.90609
6.1549U
6.41177 ...
6.67251
6.92930
7,17818
7.43496
7.69965
7.95644
8.20928 	
8.46606
B. 71890
8.9677H
9.21667
9.43396
9.65519
9.90407
10.14506
10. 38209
10.61913
10.85617
11.CV320
11.44085
11.89517
12.'34553
12.74985
13.^4626
13.69470
14.11539
14.5I8IU
14.')t>477
15.37950
15.7785'!
16.15388
16.51 tin
l6.8hU9)
17.2lt5H
17.1oO?9
17.9UU04
III./ JIH-I
111.5-iSlll
III. I1797H
l').l'!5H2
I9.5019/
I'l.lU'lll/
/0.10K4I
2U.4C471
2C.((''/05
,'0.'if/'>4
<•!.;• '>Mill
21.->t'.'/o
tl.H'iSt.
CC/MIN
t
.
DIFFtKI-NTIAL R4Tt
MOM ACID/CM C-MIN
1.10616
0.94810
O.B6913
0.06913
O.B6913
0.8691 1
0.79016
0.79004
0.86913
0.86913
0.94822
0.63199
0.7112C 	
0.86913
0.79004
	 O.J9016 	
0.71107
0.79016
0.79004
0. 869 13
0.94822
. 	 .0..86913 ..: 	
0.86901
0.86913
_ 	 _._0.«.8t9l 3 	 _...
0.86913
0. 79016
	 0..86913. 	
0.79016
0.84277
	 0*89545 	
0.84281
0.84277
0.86913
0.86913
0.84261
0.34277
0.81645
0> C*t2t> 1
.0.86913 	
0.86913
0.84277
C. 81645
0.89545
O.B6913
_ 	 0.84281 	 ._.
0.84277
0.86913
0.81645 	
0.84281
0.81645
0.63211
0.84277
0.81645
0.79012
C. 79012
0.79012
0.79012
0.79008
0.76378
0.75062
0. 75060
0.76370
0.72428
0.7)744
0.69793
0.71112
0.71109
0.67161
0.65R4 »
0.59258
O.o0'i74
0. 5/942
0.5/042
a. 56624
0.56626
0.5»'"*2
0.5 i9'fl)
0.53'l'»2
U.51 157
0.->l 1S7

-------
C»ltUl»l IDNi MIR bkAVIMtIkIL  ILIIW I I l>l ft I Ml Nl !>
RUN NO. • l»9
UAIt • 8 31 71
MY NT.- 98.86 MG
CUKKECIIUN- -6.27. MO
MEAN LOAD
GKS~S02/100 GKS C
0.31687 	
0.48160
(j. 5988V
0. 69371
0.77856
0.85341
0.93077
1.01811
1.10296
1.16201
1.26266
1.34251
1..419B1 	
1.49971
1.57958
	 1.65443 . .
1.72680
1.B0166
	 . 	 1.67403. 	
1.9)641
2.00129
	 2.06617
2.12607
2.18096
	 2.230J7 	
2.28078
' 2.31068
	 2.38059
2.42801
2.53780
.2.70998 .
2.87468
3.03189
j. 18410
3.336)2
3.48605
?-*'*;>;»''
i. TU 300
1.93023
4.07496
4.21969
4.36442
	 4.50666 . .
, ' 4.64391
4.78365
4.925S9
5.04816
5.1729}
	 .5.31517 	
5.45740
i. 59714
5.73439
5.B74I3
6.011)6
6.14B62
6.28587
6.42312
6.55787
6.68763
6.87229
/ 7. 12682
7.39632
7.66083
7.91785
8.17238
8.42691
8.68144
8.92849
9.16804
9.40760
9.64965
9.89669
10.14)74
10. in 1,29
10.625)4
I0.867*>0
Il.0'l4t8
11. 1/406
l|.M8f>6
11.74577
11.91.0 IB
12. 11/49
U.lMoO
li.s-UM
I.'. /Ill 16
I/.976UO
1 1. l«,5f.5
1 1. 3Vi««)
| i. *> \'t'tt>
5I>2 • 2000. fl'H
NO • 150. PPM
02 - 3.i J
M2.D •.... 6.0 < 	
DIFFERENTIAL RATfr
MGK S02/GM 0-HIN tMS
	 1,54713
1.34751
0.99U14
O.R983H
0.798',7
0.69870
0.84650 	 ..
O.B9U30
0.79B54
	 0.79854
0.79H47
0.79854
0.74U66 _
0.84(i76/
0. IS7<,«
0. 14') JS
0. 14IU4
0. 11/71
. . O.JI271
0. llhU7
0. Ul.U'l
0. «>' "'
0. II Ml 1
7CHP • 700.
Fill T.C/C.
H2S04 " 75.55

HttH ICIAU
At ID/ 100 CMS C
0.51581
0.7174t.
0.91705
.06225
.19216
.30679
.42525
.55899
.6889U
.81118
.93345
2.00572
2,17418
2.29645
2.41873
2.53335
2.64416
2.75879
	 .2 ..869,6] 	 	
2.96513
3.06448
3.16383 	
3.25554
3.3)960
_ . 3.4160.2. 	
3.49244
3.568H6
3. 64528
3.7178b
3.86601
4.14966
4.40186
4.64258
4.87566
5.10875
5.33801
5.56345
5.79272
6.01116
6.23978
6.46140
6.68302
6.9008?
7.11098
7.32496
7.54276
7.72999
7.92104
' ,8...UOa5 	
' 8.35665
8.'57063
" 8°". 7807B
" '8.99476
9.20492
9.41506
9.62524
9.83540
10.04173 	
10.24043
10.52119
10.91294
11.32561
11.71064
12.12421
12.51196
12.90370
11.29345 	
13.67174
14.01856
14.40539
14. 77603
15.154H
15.52876
15.89942
16.27005
16.61)04
l6.V.1t>47
I7.JJVJV
17.(.6H'>&
1/.')')0
0.5094/
0.54761)
P. 54770
O.M49S
0.577/7
P.su*).. 7
0. S094'*
0.4H1'I'»
0.4H4U1
0.47U6
U.4U4UI
                   488

-------
          CALCULATION'.. FIIK GKAVlMttKIC  film
IUT-7-6C-4
 .RUN NO.  •   191
     U»U  «   9  2 71
   (IHV nl.-  100.56 HC
CCHKEUlUN*   -6.43 HC
                            S02 •  2000. PPM       ICMP
                            HO *   ISO. PPM       Fit)  »
                            01 *    3.5 t        II2S04  •
                           1120.-	6.Q.I		
                                                     200. DEC. F.
                                                   1500. CC/KIH
                                                   76.20 (
   ..HE AH LOAD
CMS SU2/100  (.MS  C
                      PIFFCHENUAU RATE
                      M(iM !>02/GM C-HIN
                                        MEAN  LOAD
                                    CMS ACID/100 CMS C
                 DIFFtRCNTlAl PATE
                 MOM  ACID/CM C-MIN
3.35629
0. 47011
0.57156
0.66063
0.74476
IJ.B2394
0.89B17
0.96745
1.03425
;.-. 1.10106
1.14312
1.U51B
_ . .. 1.24704
1.30147
1.35143
- .-. 1.40539
1.454BH
1.50189
	 1.54643
1.59097
1.6)796
1.6H499
1.72705
1.76911
. 	 .- . 1.81366
1.65572
1.69283
	 1.92747
1.96459
2.05119
?r 17490
2.29119
2.40748
2.52378
2.64007
2.75141
2.R57B1
2.96421
3.G7U6U
3.39720
3.38216
3.46628
. . 3.58773
3.68917
3.79062
3.BB960
3.96857
4.0B754
4.27006
4.36961
4.46116
4.55518
4.64921
4.74076
4.82963
1.91690
5.C0796
5.14159
S.690H9
S. 117 199
6.05214
6.227H1
6. 564 12
6.71217
7.0b41 1
7.22741
7.3H579
7.54167
7.H64HO
f. 14 1 14
P.H0604
	 1.18762
1.0BB70
0. 94025
. O.B4126
O.B4126
0.74234
0.74226 	 	 _
0.64334
0.69200
0.64334
0.19764
0.64334
0.5918)
0.49489
0.54435
. 0.494B2
0.49439
0.44536
O.44S16
0.44543
0.49402
fl. 44536
0.39590
0.44536
	 	 	 0.44543 	 	 _..
0.39590
0.34636
	 0.34644
0.39590
0.44536
0.37941
0.39587
0.37939
0.39590
0.37939
0.36290
0.34641
0.36290
0.34039
1.63099
0.34641
0.34641
... 0.32990 ... ..
0.34639
0.32993
0.32990
0.32990
0.32990
0-JI 14.?
0.31342
0.'29690
0. '3 1 342
0.31342
0.31342
0.29690
0.29693
0.29690
0.29691
0.29692
0.10516
0.30516
O.U 142
0.296V2
0.29692
0.^(1867
0.2H04?
0./6B66
0./I21II
0.2/2U
0.27218
0.25S6B
0.26393
0.27216
0.27218
0./63'*J
0.2619?
0.26 I'll
0.2556B
0.^.4557
0.719B5
0.87520
1.01159
1.14041
1.26165
1.37532
1.48140
1.58370
1.68600
1.75040
l.dl4BO
1.99288
2.07244
2.15201
2.22778
?. J6796
2.43616
2.50815
2.58013
2.64454
2.70695
2.77715 	
2.64157
2.8984G
2.95144.1..
3. (0628
3.14088
3O3032
3.50834
3.68646
3.b6453
4.C4260
4.21310
4.37602
4.53894
4.70185
5.20197
S. 17924
5.33837
5. -.9371
5.04905
5.60439
5.95594
6.10749
6.25904
6.55078
6.69096
&. 83115
6.97512
7.119.10
7.25"92B
7.3^567
7.53207
7.66647
7.67307
8.14965
8.4'iOOl
8'.71417
*'.99454
9.26713
9.53634
9;797/7
10, (5162
10ilJ925
10.'>b(.8ti
lO.tl'694
11.06701
11.30'9'.9
11.54H1U
12.C-.4Sl
12. SI 326
12.77574
1J.U1444
13. .'4914
1.B1854
.66707
.43975
.28817
.26617
.13670
.13659
0.96512
1.06085
0.96S12
0.30294
0.98512
0.90927
0.75780
0.83354
0.757W
0.75780
0.68195
0.68195
0.68207
0.75769
0.68195
0.60622
0.68195
._ 	 0.66ZQ7 	
0.60622
0.53037
.. 	 	 C.S3048._ 	
0.60622
0.68195
Q. 56097
0.60618
0.58094
0.60622
0.58C94
0.55569
0.53045
0.55569
0.53041 .
2.60370
0.53045
0.53045
0.50516
0.53041
0.50520
0.50516
0.50516
0.50516
0.47992
0.47992
0.45464
0.47992
0.47992
0.47992
0.45464
0.45467
0.45464
0.45467
0.4546'.
0.46726
0.46728
0.47992
0.45465
0.45465
0.44203
0.-.2939
0.41677
0.44201
0.41677
P. 4 167V
0.41677
0.391SO
0.40416
0.41675
0. 416/7
0.4041'j
0.40413
0.4041S
0.39150
0. I11"i0
0. 19150
1. lU'.ll
4.24H94
'l.i'ljlt.
     : III
                             0.24 (41
                             0.24(41
                             0./101S
                             0.^4 1-1
                             U./t 1- I
                             U.I t'MII
                             U..MOO
U./I1)'*

14.16245
14. JU2.'U
                                                                      0.3(811(1
                                                 lt.-.-4'tU.*
                                                                      0. IS 164
                                                                      0.3/HUU
                                                                      (>. IMIUH
                                                                      0. 1
                                                                      0. 1
                                   489

-------
         C«lLlll»I KINS till- I.MAVIHI tUIL Him  I
mr- /-M.-5
•UN NO. • 1<>2
UAH • '1 )
0»» 1,1.- 100.90
CUK«f.<.I| UN- -6.U
MEAN 1040
OKS SU2/100 i,HS C
O.TJSOS 	
0.94471
1. 14060
I.2II6BH
1. 42574
I.5U939
1.74064
1.B7950
2.00B4)
2.1 J489
2.25dB7
2.3/789
2.48947 ...
2.59609
2.7U5I9
2.81181
?. 910<)V
3.01010
3. 1G936
3.20606
3.3002H
3.38707
3 . 4 6 « 8 9
3.5556B
J. 63993 _..
3.71933
3.80J6J
- . J. 69042
3.97472
4.I4S29
'..19073
4.63677
4.97480
5.11532
4.34096
5.56660
i.B096J 	
6.05011
6.2B071
6.50e3'i
6.73440
6.95763
7.23039
T. 45355
7.62711
.. . f. 64780
6.06000
It. 28172
	 8.')
ll.fJ.??!
IP.i'OdSA
12. S*^?
L'.bH 11
13.2.IHM
1 l.".ti:lilu
1 1. 7r.',J I
l<>*> t
1'.. JS>.|I.
l<..6U)^
l't.91 4S'»
I4*. lt^f(.'
l'i.*.4 If, 'Ml
llt.f.// .',
I r>. N'htl<>
II. II Oil/
17. ) 1 IV.
I I. •>•,.' MI"
I 7. / lii/s
1 1.10'IB'.
ll ,(l'..l'..,
l-,./-.'l 1
| I..IM,.-.
sn? « 2000. n>x
71 NO ' 140. PI'M
HO 02 • 3.4 \
ft> H20 «. 6.0 t
DIFFERENTIAL RATE
RjM yj2/f.M C-H1N CMS
„ 2.18202 _.. 	
2.03326
1.H84U
1. 04 13 7
1.73S6>
1.53139
1.48768
1.2U942
1.28934
1. 23978
1.23'J7S
I.140i«
1.09101
l.U4l4'>
1.140S8
0.99161
0.991BS
0.99161
0.-)9161
0.94225
0.94225
0.79340
0.84304
0.8926B
0.79348
0.79340
0.8926U
	 0.64304
0.84304
0.87611
0. 19348 _ 	
0.79345
0.79345
0.61000
0.69427
0.81000
0. <1C9'<7
0.79345
0.7' 389
0. 17693
0.72732
0.76041
1.057V4
0.429 It
0.727)4
_ 0.7.43S6 	
0.71002
0.7273*.
O.S9510
0. (6038
3.69427
0.67775
0.66123
0.66121
0.66121
0.66123
0.64468
0.64468
0.6446(1
0.62815
0.62816
0.5H082
0.57U56
O.i/OJO
n.->6204
0.n->377
0.5)721
0. 1967 t
J.'>2l)/l
0.*.H 7o4
O.I, III.'
0.462«'>
11.471 12
0.4.-97H
J.'* tHtl1*
3.*/lll
0.4D4T*
0.4 1 !.'<.
:1. IHu4 /
0. VHi/o
0. IVi'i>)
i>. tf.[l«"l
ll. I1.'.'. 1
0. *.'.' t-.
0. t H'OI*
0. / \'tt,-t
ll.,1!!'*/ 1
!>. ,'t. I.1 /
0. .' r'l,' t
rrup • 200.
Fill * 15CO.
H2SU4 • 76.62

MEAN 1010
AC1U/100 GHS C
	 I.J23.86 	
1. 44659
1. 14654
1.97054
2.18316
2.43375
2.66536
2.b779d
3.07541
3.26905
J.45U89
3.64114
3.81199
"3.975JO
4.14232
4.30558 	
4.45746
4.60934
4.76121
4.90928
5.05356
5.18645
5.31174
5.44463
._ J. 57373 	
S. 69522
5.02431
5.95720
6.08629
6.352C7
. 6./J556
7.10005
7.46454
... 7.832U4 	 . 	
8. 17835
8.52386
B.a9>95 	
9.26424
9.61734
9.96660
10.31216
10.65388
11.07154
11.41324
11.679C2
12.U1694
12.35106
12.68139
12.96514
13.29647
13.63059
13.94572
14.25327
14.55702
14.86076
15.16451
15.46446
15.76061
16.05676
16.49339
17.07051
17.62865
18.16400
10.69176
19.21191
19. F2450
20.2251-8
20. 61.471
21.1/616
2l.'»19U
21 ,'i;tiHO
22.406h6
22.KWB9
23. .517-.
,' (.(-'.041
.'4.1.4S2'!
24. '4/4.11,
4>4.l',0i/l^4
2*>.lii'HI
."•.VI.-D
2-1. III1)!1)
/I...-1 ».'i.
21, .•>'. 1 111
.'(•.rl,<">2
.'I.I(.2'.6
2l.'t.'44'.
.' / . 1, 1. / , •»
27. iM.M
211. 1 r».-l
[Jf&. F.
tC/MIN
t

OlFFfRfNTIAl RATE
K0« AUD/&K C-M1N
	 3t>4123 	
3.11343
2.B8551
1.59460
2.65771
2.35413
2.27800
1.97442
1.97431
1.89841
1.B984I
1.74651
U67061 	
1.59472
1.74651
	 J. 5187.1 	
1.51882
1.51871
1.51871
1.44281
1.44281
1.21490
1.29091
1.36692
>. 21501 _
1.21490
1.36692
	 1-.29Q91.. 	
1.29091
1.34154
1.21501
1.21497
I.21A97
1.24031 	
1.06311
1.24031
	 _l. 24027 _._ 	 	
1.21497
1.1390D
	 L.169>t 	
1.11370
1.16438
	 l.._61?9B 	
0.65810
1.U374
1.13904
1.08844
1.11374
0.91124
1.16434
1.66311
.03781
.01251
.01247
.01247
.01251
0.98717
0.98717
0.98717
0.961B6
0.96187
O.H9857
O.H8592
O.H7327
O.B6062
O.B4796
0.82264
0.6U7*9
0. 79734
0.74670
0./2I41
0./CU/4
0.72141
0.65810
O.blOl/
0.64547
0.62014
O.M2HO
O.S94D4
0.60T5I
O.H4420
0.-.8219
0.54420
0.4'J>'>9
0.50625
0. 16/02
0.-.429I
0.4429S
(l.442'<7
                               490

-------
         CALCULATIONS FOR GfUVlHtfHIC FLOW
R«f-7-6C-6
RUN NO. - 193
DATE • 9 7 71
I>RY 1.1. • 10?. 82 MG
CLRKECIION- -6.lt) MC
HtAN IUAD
CMS S02/100 CMS C
0.36777
0.49601
O.blVil
0.7)797
0.85895
0.9(509
I. 06461
1.15172
1.22)76
1.3*719
1.45659
1.55095
1.64290
1.73242
1.81464
1.89454
1. 97661
i. 05907
2.13650
2.20909
2.26409
2.35668
2.426B5
2.49460
2. 56235
2.63252
2.69543
2.7SB33 . .
2.82366
2.95190
i. 14063
3.32210
3. 49673
3.67778
3.66168
4.03831
4.21252 ..
4.39157
4.56578
4.73999
4.91178
5.08115
	 5.25052 	
5. 41990
5.62556
	 S.B2B81 	
6.00302
6.17723
	 6.34902
6. 52124
6.69261
6.86198
7.0313S
7.19589
7.35000
7.51770
7.67497
7.82982
7.9H46H
6.21444
8.51699 .__
8.79524
9.06382
9.34449 _
9.6?0i)
9.6X690
10.15506
1 (>.4IBdO
IC.6H25I
10.94627
ll.2U2r5
1 I.4S1 19
11.70361
II.9S2B2
12. ll'Jl
12.4143)
12.6«'I01
12.901 H
u.um
1 >.3*>6I9
l).V.'M2
1 !.7(VO'>
1 l.'I'IOl 1
14. I'IMIll
14. 196*1
|4.S'I74'.
I4.nl>ll(u
14. -Mlifc'l
I'..!'. 'H 1
SCI2 • 2000. ffH
NO • 150. PPM
02 • 1.5 *
H211 • 6.0 I
liIFFFRFNIIAl KATC
UGH S02/GH C-MIN CHS
1.25824
1.30653
1.16144
1.20980
1.20980
1.11300
0.67749
1.06463
1.01626
1,01619
0.967B.)
0.91946
0.91446
0.87110 	 "
0.77422
0.82273
0.82266
0.82266
0.725B5
0.725V3
0.77422
0.67749 . .
0.72593
0.62905
0.72593
0.67749
0.5B068
0.67749
0.62912
0.64522
0.61297
0.5968)
0.58071
.. . 0.61297 _
0.61297
0.56456
0.59685
0.59663
0.56456
-. 0.59685
0.54844
0.56071
	 0.54844 ....
0.58071
0.79041
0.56456 	
0.596*5
0.56456
0.5B071 	
'0.58071
0.54646
0. 58068
0.54846
0.54U44
0.53232
0.53232
0.51617
0.51619
0.51617
0.50812
p. 50005
0.42746
0.46779
0.46779
0.45166
0.44360
0.44 )60
n.*)')^?
0.443M)
6.4»55i
0.419J')
0.41940
0.41133
0.4194U
O.J9521
0.395 14
0. Jtt71*>
0. IH711
0.38713
0. I-.4IID
0.3'>40ll
0.3VHIU
0. Jill 74
0. 14(>l.O
0.12262
0. *4bHO
n. i ii'Mi
0. l.'/til
0. t|4'l'i
TtHP =
FID •
M2SU4 •

MCA^ LOAU
ACID/100
0.5631)
0.75951
0.94847
1.13001
1.31526
1.49310
.1.63019
1.76357
1.92289
2.07850
2.23040
2.37489
2.51569
2.65277
2.77874
2.90101
3.02699
3.15296
. .3.27151
3.3e266
3.49752
3.60866
3.71611
3.81985
3.92359.
4.03104
4.12737
. 4.22370
4.32374
4.52010
4.80909
5.08697
5.35743
5.63160
5.91319
6.18365
6.45042
6.72459
6.49134
. 7.25811
7.52116
7.78052
8.03987
8.29922
8.61415
8.92536
9.19213
9.45889
9.72194
9.98670
10.24806
10.50741
10.76676
11.01870
11.26694
11.51147
11.7522V
U.98942
12.22653
12.57851
. 13., 04164
13.46772
13.87897
14. JOB76
14.73113
15.14238
15.5444*
15.95370
16.35,762
16.76147
17.154?!
17.53902
17.42114
lt>.302'*>
I8.6f69»
1t<
20.77771
21.10.»H
21.422 H<
2 1 . I il \a
^;. 04483
2.'. t'u' 14
2,'.6M'-[.
2..VI. Jl.f
i l.,">ti ll.
200. UfG. F.
1500. CC/H1N
76.19 t

UIFFEKENTUL RATE
CMS C "OH AC10/GM C-MIN
. . .. 	 1.92668
2.00063
1. 77845
1.85251
1.65251
1.7042B
	 .. 1.03740 .
1.63021
1.55616
1.55604
1.48198
1.40792
1.40792
1.33386
1.18552
1.25980
1.25969
1.25969
1.11146 	
1.11157
1.18552
1.03740
1.11157
0.96323
1.11157
1.03740
0.88917
1.03740
0.96334
0.98799
. . 0.93862
0.91389
0.88921
	 	 0.93662 	 . ..
0.93862
0.86448
	 .._.. . 0.91393
0.91389
0.06440
	 	 ... 0.91393 	
0.8397S)
0.86921
... 	 0.83979
0.88921
1.21032
. 	 0.86448
0.91393
0.1)6446
._ . 	 O.B8921 . ....
0.88921
0.63983
0.88917
0.83983
0.83979
0.81511
0.81511
0.7903B
	 0.7904?
0.79036
0.77B06
0.76570
0.65455
0.71631
0.71631
0.69160
0.679/6
0.67926
0.6bf>89
0.67926
0.66691
0.64219
0.64221
0.629H5
0.04221
0.60516
0.60514
0.19?B.'
O.VI2HO
0.542BO
0.-.4 141
0.44141
0.54341
O.MH70
o.'.jio'.
0.49401
0 . '» 1 1 U4
P.'.OI', Ih
0,4'( »/•)
O.irtll '•
                            491

-------
         C4lCUl»IIONi Ft)« GKAVIHllKIt
                                        IHI'tRIMtNl!,
R«T-7-lt-7
RUN Ml. • 194
DAM • 'I 1 71
DRY Hi." 10). JO HG
COHftfU ION* -5. 911 KG
MEAN tO/10
CMS SU2/100 CMS C
0.7)929
0.782)6
0.82781
0.87567
(<.v2)52
0.97)76
1,02400
I. 07*2',
1.12210
1.160)8
1.19627
1.23455
_. 1.27522 .
1.3I82U
l.)49)9
1.37810
1.41876
1.45945
1.49773
1.5)601
1. 57479
1.61257
1.64846
1.68195
1.71)06 ._. .
I. 74416
1.77287
1.60398 ...
1.8)747
1.89250
1.97624
2.06237
2.14611
2.22507
2.30402
2.38298
2.45954
2.5)849
2.615C5
2.68444
2.75143
2.82081
2.89020
; 2.94719
3.02418
_, 	 J. 08878 	
3.15337
3.22037
	 3. 28497 . .
3.34717
3.409)8
1.46919
3.52901
). 50600
3.66299
). 72159
3.79219
	 ). 854)9
1.91899
4.01469
4.13671 _
4.256)-<
4.37597
. .4.50039 	
4.62958
4.756)9
4.B7B4]
4.99804
5. 11766
5.2)968
5.36170
5.4UI »
5.59857
-,.71341
5.825H6
5.93VU
6.04 I5H
6. |4llO->
6.2517J
6. 14 'III j
(I.445S3
6.5)11 114
f,.l,)?|->
6. 7U4?
0. IK. 001
i..'f4Ssn
It (,Mli'i
f.lM>-'0
r./i-isr
so? • 2000.
NO « ISO.
02 - 3.5
K20 * 6.0
DtFfeRfNIIftl RATE
«GM S02/GM C-M1N
0.43064
0.43064
0.47854
0.47U47
0.47054
0.52636
0.47847
0.526)6
0.43G72
0.13492
0.362U2
0.3S2S2
	 _ 0.4)064
0.43064
0.19145
0.38282
0.43064
0.38282
_.. .O.JB282. _. .
0.3828?
0.38274
0.38282
0.3)499
0.33492
0.2871/ 	
0.33492
0.23927
0.38282 _
0.28709
0.27M5
0.21)712
0.28709
0.27115
0.25521 	
0.27115
0.25521
0.25521 	
0.27115
0.239^5
. 0.22JJO ....
0.22330
0.23927
. . 0.22)30 '
0.22330
0.223)0
- 0.207)4. _..
0.22330
0.223)0
.0.20736 .„_
0.207)6
0.207)4
0.19142
0.20734
0.2)927
0.207)6
0.22330
0.207)4
. 	 0.20736
0.2D30
0.20O5
	 0.19936 .._.
O.IV938
0.199)8
_. 0.21S))
0.2153)
0.20735
0.19938
0.199)8
0.19v)U
0.207)5
0.199)8
0.199)8
0.19141
0.19141
0.111 14)
0.18)4)
0.17545
0.17545
0.16740
0.15950
0.1VI50
0.1515)
0.15'l-jU
d.l'll4l
O.lbNr
0. IhHtl
O.I HI-. I
O.IH)-,)
0.1 7-J4S
PPM IfMP • 200
PHH Mil • IV-iO.
< H2&L4 • 75.64
(
MEAN LOAD
CMS AC1U/100 GMS C
1.1320S
1.1979U
.26759
.)40U6
.4141)
.49107
	 	 	 .. .56800 	
.6449)
.71821
.7768)
.81178
.69040
	 	 .95268 .. .. .
2.01862
2.06675
2.11022
2.17250
2.2)476
	 2.29340
2.35202
2.4106)
2.46925
2. 52420
2.575»9
2.62312. . ...
2.67075
2. /1471
2.76234 . 	
2.8136)
2.89789
3.C2612 	
3.15801
3.2862)
3.4071) ......
3.52803
3.6489)
3.76617
3.B117C7
4.004)0
4.U054 	
4. 21312
4.319)7
4.42562
4.52820
4. 6307 H
	 4.72969
4.82860
4.9)118
	 	 - 5.0)010 . 	
5.12536
5.22061
5.31220
5.40)79
5.50637
5.60896
5. 70768
5.60679
.... _. 5.90J04
6.0009A
6.14750
... 	 6.))43.4__ 	
6.51752
6.70070
6.89171
7.08905
7.2t>322
7.47006
7.05)24
7.tf)642
8.C2326
8. /lull
».)-»J29
8.57280
8.74866
8.-J20HS
V.Ob'IU
<).2IJ42)
9.4154)
9,1/2'((
4
IU.6IS41
10. Mix, I
10. "1. '.I)
1 1.1 HUH.
. DEC. F.
LC/HIN
i

D1FFERCNT1AL RAT6
MC.M HCIU/uH C-HIN
0.65942
0.65942
0.7)276
0.7)265
0.7)276
0.80600
0.7)265
O.U0600
0.6595)
0.51285
0.58619
0.58619
	 0.65942 	
0.65942
0.29315
0.58619
0.6594?
0.58619
0.58619 	
0.58619
0.58608
0.58619
0.51296
G. 51285
0.4)973 	 ..
0.51285
0.366)8
	 0..58619
0.43961
0.41520
_ 0.4)965
0.4)961
0.41520
. . O.)9079 .. _ .
0.41520
O.)9079
O.)9079 	
0.41520
0.366)S
	 0.34193 .. 	 	 _
O.)4193
0.36638
0.34193
O.)419i
0.34193
O.)1749
0.34193
0.34193
	 O.)l752 . 	
O.)l752
0.31749
0.29311
0.3174S
0.366)8
O.)1752
0. 34193
O.)l749
O.)175?
0.34193
O.M751
0.30530
0.30530
0.)O5)0
0.32973
0.)2973
0.31751
O.)05)3
0.30530
0.305)0
0.31751
0.305)0
0. 105)0
O.?9)0<)
0.29)09
0.28087
0.280S7
O.26H67
0..'6D67
0.25646
0.24424
0..'4424
O..')20)
0./4424
0. ."*)»')
O.J'i64'.
(<..">646
o..'iiiiur
o./iii'iir
C. .'tiHt*/
                              492

-------
         CALCULATION!!  rim (.RJVIHICRIC  HUH KPCRIMINIi
KT-7-6C-8
RUN Nl). > 19i
U»H • 9 10 71
DRY HT.» 104.70 MC
CURRECIIUN' -5.87 HO
MEAN LUAD
CMS SO// 100 CMS C
0.489 16
0.5H292
0.66689
C. 74165
0.81802
O.BH999
0.9'.,716
1.019%)
1.00190
1. 14187
1.19705
1.24983
1,27861
1. 10740
1.36017
1.41051
I. 4585)
1.50651
1.55681
1.00726
I. 65284
1.6936)
1.7)6111
1. 78478
1.830)7
1.0711%
1.90953
1.95271
1.49829
2.06225
2.20460
2.J2454
2.44449
'2.56444
2.684)8
2. 8019)
2.91948 ..
3.034ft}
3.147)7
3.26252 . 	 ..
3.37527
). 48802
3.60077
3.71352
3.82627
	 3.93902
4.05176
4.16211
	 4.27247
4.38262
4.50036
4. 61551
4.725R&
4.83861
4.9489h
5.0593?
5.16966
5.28001
5.38797
5.54869
5.76460
5.9H290
6.20360
6.42190 . ;._ .
6.6)041
6.84651
7.0'-2H2
7.2S43)
7.45B24
7.hf>451>
7.U/OKI.
8.072)7
II.26-JOI)
8.4W
0.6?4*>0
tl.K 71140
•i.nos:
V.//IX, I
9.4/C"»4
v.M..'tlfi
9.7
10.0I'<4«
ll<./>/Wll
10.41141.'
lU.5l>4Ci
l|i.7M'>r>
ll'.'M4,">
11. 1 .".'.. I
II.//OI*
S02 • 2000. t>t>H
NO » 150. PPM
02 • 3.5 %
H2tl - 6.0 X
01FF[ftf:NTIAL RATE
KCH S02/CH C-MIN CMS
0.95955
0.91160
0.76767
0./6767
0.71965
0.71972
0.62367
0.62374
0.62374
0.57572
0.52777
0.52777
0.04795
0.52777
0.52777
0.47981
0.47974
0.47981
0,52.117.
0.47974
0.4)106
0.38)84
0.47974
0.47981
0.43179
0.3&.)»4
0.}8)b4
0.47974 _..
0.4)186
0.41580
0.399U2
0.39982
0.39982
0.39982 _ . . .
0.39962
O.J8)64
0.39982..
0.36783
0.38384
0.38381 	 - .
0.36783
0.38)84 .
0.3678) 	
0.38)84
0.36783
0.)8384
0.36783
0.367(f3
0.36785 	 	
0.3678)
'0.41500
0.35164
0.3D3H4
0.3678)
0.36765
0.367B3
0.36783
. 0.16783 	
0.351B4
0.359H4
. 0.35VU5. 	 	 _
0. 16781
0.367D4
0.359B4
0. 15184
0. 151114
0.335115
0.3)5i>6
0. I4J84
O..I4 3HS
0. I41U4
0. )2 tan
0.3^7U6
0.343H4
0. )15l)'>
0. 14 *ri5
0. 127(16
0. *2'H4
O.J1906
0.11 'HIS
0. U 1M,
0. U1U6
0. I0)x;
P.."<'jll(>
a.)otvt
Q..'HIHl
0. ,'lt /I) /
O.^'/'/l'M
{l..''l«ll
TEMP • 200.
Fill • 1500.
H2S04 • 76.92

MEAN LOAD
ACIU/100 &Ki C
.' 0.74.9)4
0.89260
.02117
.13872
.25259
.36279
.46565
.56115
.65666
.74B49
.8)298
.91379
.95787
2. 00195
2.08217
2.15991
2.23)37
2.3U6B4
-2.3»39fl . .
2.46112
2.53092
2.593)7
2. 6594(1
2.73295
2.80275 	
2.86519
2.92397
2.99008. 	
3.05988
3.18845
3.37579
3.55945
3.74312
). 92679 	 	
4.11046
4.29045
4.47045
4.64677
4.61941
. .4.99574 	
5.1663d
!>.)4103
..5.51)67 	
5.68632
5.85697
6.03162
6.20426
6.37324
-6.54221
6.71119
6.89118
7.06750
7.23648
7.40912
7.57BIO
7.74708
7.91605
6.08502
8.25032
8.4964)
8.82704
9.16111
9.49926
9.H3)'>4
10. 16047
10.4S372
10.79963
11. Kit A:
11.42044
11.71614
12.05225
12.360K)
l2,t>b2U3
l2.'i(OVI
1 .).<•«, 3 J
13.59506
1 1. /OJl'J
14.204h4
U.502IH
14. Ml.25
15.0Bli44
l'>.SI/-lt,
IS.dS1)!!!
|5.»ll II
t6./y6nj
t6.4 ttU'1
II../4 >!.'
l/.i'vl)1'.'
I/.2'. />•(
Dtr,. F.
CC/KIN
I

UlfftRENTIAL RATE
KC.K ACiu/cp C-MIN
- _L. 46932
.395119
.1/550
.17550
.10196
.10207
0. 95499
0.^5511
0.95511
O.tol-,7
0.80814
0.80814
0.07343
0.80814
0.80814
0.7)472
0.73460
0.73472
0.8U814
0.73460
0.66129
0.58775 . ._..
0. 7)460
0.73472
0.66118
0.58775
0.58775
	 0.. 7 3460
O.D6129
0.63670
0.61223
0.6122)
0.61223
.__ 	 0.61223
0.61223
O.D6775
0.61223 	
0.56324
0.56775
	 	 .0.58771 ... 	 	
0.56324
0.58775
0.56324
0.58775
0.56)24
0.5S775
0.56324
0.56324
	 . 0.56327 	
0.56324
0.6)670
0.53676
0.58775
0.56324
0.56327
0.56324
0.56324
0.56324
0.53876
0.55100
0.55102
0.56)24
0.56)26
0.55100
0. 5)876
0.51876
0.51427
0.5142'!
0.5/650
0.526'.2
0.52650
0.5020)
0.50201
0.52650
0.51427
0.52hS2
0.50?C)
O.S020I
0.4H9/9
0.4n'l7f
0.417'.)
0.4/751
C.46MO
0.45104
0.46S30
0.440110
P. 4411 III'
C.4.'H'>7
U.4I611
                            493

-------
          CALCUUUONS FUR GRAVIMtrHIC  FLOM

a«r-7-6C-»

  BUN NO.  •   l">6           SU2 •_ 2000,  PPM  	 TfMP «_  200. PEO.  f.
     OAlf  •   9  14  71       140 «   150.  PPH      Fill *  1500. CC/MIN
   OdY WT.-  100.42 HC      02 •    3.5  *      H2S(K '  75.78 *
*EAN LOAD OlFf EfUNTIAL RATS H6AH LOAD . .. DIFFERENTIAL RATE 	
iKS S02/100 SHS C KGM S02/GM C-MIN CMS ACID/100 CHS C MfcH ACIU/GM C-MIN
n.4tftAq O.49?R590
1.20363
1.24136
1,2790?
1.31305
1.34324
	 1.J7719 _.. 	
1.41493
1.45266
1.4«662
1.52057
1.55453
1.58472
1.61490
1.64836
1.68262
1.71301
1.76582
1.84506
1.93184
2.01862
2.10163
2.18464
2.26387
2.33933
2.414UO
2.49026
._ 	 Z..5657.3 	 	
2.64119
2.71665
2.79212
2.86758
2.94304
3.01850
3.09019
3.16188
3.23357
3.30149
3.36941
3.43732
3.50147
3.56184
3.62590
3.69012
3.75427
3.61841
3.90897
4.03725
4.17309
4^30892
4.44098
4.576BI
4.71642
4.85225
4.98809
5. 12015
5.25598
5.39182
5.92387
5.65593
5.78799
•i.9238)
6.05589
6.18795
6.32001
6.44630
6.57281
t.6'1732
6.82561
6.95)89
7.07841
7.20292
— .. 7.J31Z1.
7.4557?
7.50024
	 7.f04,T6 	 	
0.402/6
0.37734
0.45276
0.45276
0.37/34
0.45276
0.37/34
0.37734
0.45276
0.45276
0.45276
0.37734
0.37V34
0.37734
0,37722
0.30192
0.301110
	 0,37/34 	 	 _.
0.37734
0.37/34
0.301(10
0.37734
0.30180
0.30192
0.30189
0.37734
0.30192
0.30180
0.25156
0.27670
0.30184
0.27670
0,27670
0.27670
0.25152
0.25156
O..O156
0.25152
0.25156 _
0.25152
0.25156
0.25156
0.25152
0.25156
0.25152
0.22643
0.25152
0.22&38
0.22642
0.22638
0.22638
0.20124
0.20124
0.2263B
0.20124
0.22638
0.20124
0.20124
0.22638
0.22640
6.22638
0.21381
0.23B97
0.22640
0.72638
0.22640
0.21381
0.23897
0.21381
0.22638
0.21381
0.22640
0. 22638
0.21383
	 0.226)8
0.21381
0.21381
0.20U4
0.213HI
0.213HI
0.21381
0.20124
0.21381
0.21381
0.20124
0.21381
	 O..2012i 	
                               494

-------
          CALCULATIONS FOR GRAVIMETRIC FLOW EXPERIMENTS
 R»T-7-6C

   RUN  NO.  •
     DATE  •
    DRY UT.»
197	__W>2_'	200p._PPH 	  TEMP »   200. DEC. f_.
91571        NO-   150.>PM""    Tin*1500. CC/HIN
98.30 MG      02  •     3.5  X       H2S04 >   74.7) X
          -.JltQ
     MEAN  LOAD
'CMS  S02/100 CHS C
       _PIFFERENTIALJUTE_
        MGH S02/GK C-MIN
_ _M£AN LOAD
 CMS ACID/100 CM$"C~
 DIFFERENTIAL  RATE
"MGM ACIO/CM C-MIN"
0.58831
0.61299
0.66774
0.70001
0.72980
0.76208
0.79*34
O.B2662
O.B5BB9
. ._0. 88867 .
0.92095
0.95322
. .... 0. 9830.1. _
1.01031
1.03514
.. .... 1.05748-..
1.07982
1.10464
1.15429
1.17663
1.19641.
1.21634
1.2)620
	 	 1.25606 .
1.27592
1.29578
.--1.31812
1.34046
1.36280
, 	 .1.41742
1.47203
1.52664
— .. .1.57811...
1.63090
1.68303
	 1.73268
1.78481
1.83694
... .- -1.88.90J _
1.94368
1.99829
2.10007
2.14972
2.24404
2.29369
2.38802
2.4)767
2.48732
2.53696
2.5B661
2.6)37B
2.68094
2. 72811
2.77031
2.83733
2.93166
	 ).02351_
3.11287
3.20224
3.28912
3.38097
3.475)0
3.56218
3.64658
3.733'.,
).822S)
3.90971
3.99411
	 4.08099 	
4.170)6
4.25972
4.34909
4.4)845
4.5770?
4.62215
4.71648
4.80833
4.90017
4.9H954
5.0764Z
5.16579
5.25763
5.3*203
i.*Z147 ...
0.54612 0.90085 0.83625
0.34757
0.3*7*9
0.29787
0.29795
0.3*7*9
0.29787
0.34757
0.29787
0.297B7
0.34757
0.29787
p. 29787
0.24825
0.24825
0.19B56
0.24825
0.24825
	 _ 0.24818
0.24825
0.19B<>)
0.19846
0.19856
0.19863
3.96927 0.
t.022*B 0.
.07189 0.
.11751 0.
.16693 0.
.2163* 0.
.26575 0.
.31517 0.
.36078 0.
.41020 0.
.45962 0.
.50523 0.
.54704 0.
.58505 0.
.61926 0.
53221
53210
45612
45623
53210
45612
5)221
45612
45612
5)221
45612
45612
)801)
38013
30404
.653*7 0.38013
.69148 0.38013
.72949 0.38002
.76750 0.
.80171 0.
1.8)212 0.
38013
30*15
30404
1.8625) 0.30404
1.89294 0.30415
L. 92)35 - 0.30404
0.19863 1.95376 0.30*15
0.19856 1.98417 0.30*04
O.J4B25 2.01B37 0.38013
0.19856 • 2.05258 0.
0.18204 2.08679 0.
Or|R?G4 2.170*2 0.
30404
27875
27875
0.18204 2.2540* 0.27875
0.18204 2.33767 0.27875
O.16r>5Q 2.41749 0.25342
0.1B204 2.49732 0.
0.16548 2.5771* 0.
0.165SO 2.65316 0.
27875
25338
25342
O.lBiO* 2.7)299 O.iloty
0.16550 2.81281 0.25342
0.18704 2.B9264 0.27875
0.1B202 2.97626 0.
0.18204 ' 3.05988 0.
0.16550 3.13970 0.
0.16550 3.21573 0.
0.16548 3.29175 0.
0.14894 3.36397 0.
0.16550. 3.4)619 0.
0.16550 3.51222 0.
n.l<.R94 3.58444 0.
0.16550 .65666 0.
0.16548 .73268 0.
0.16550 .80870 0.
0.16548 .88472 0.
0.16550 .96075 0.
0.1489* *. 03297 0.
0.16550 4.10519 0.
0.1*B9* 4.17741 0.
0.13240 4.24203 0.
0.15722 4.34466 0.
0.15722 4.48911 0.
0.14894 4.62975 0.
0.1*895 *. 76659 0.
0.1*89* 4.90)42 0.
0.14067 5.03646 0.
0.16549 5.17710 0.
0.14895 5.32154 0.
0-14.067 5.45458 0.
0.14067 5.58383 0.
0.14895 5.71687 0.
0.14894 5.85370 0.
0.14067 5.98674 0.
0.14067 6.1I59B 0.
0.14895 6.24902 0.
0.14894 6.)8Srtft 0.
0.14895 6.52270 0.
0.14U9* 6.65954 0.
0.141195 6.79638 0.
0.14894 6.9)322 0.
0.16549 7.07766 0.
0.141195 7.22210 0.
0.15722 7.36275 0.
0,1*894. 7.50)39 0.
27871
27875
25342
25342
25338
22806
25342
25342
2J58.P.6 	
25342
25338
253*2
25338
253*2
22806
25)42
22B06
20273
2407*
2407*
22806
22808
22806
21539
25)40
22808
2153?
215)9
22808
22806
215)9
21539
22808
22806
22808
22806
22808
22806
25340
22808
24074
22806
0.14895 7.6*02) 0.22808
0.1*067 7.77)27 0.21539
0.15722 7.91011 	 0.2407*
0.14BV4 8.05075 0.
0.132*0 8.17999 0.
.__ 	 0.1)i40. _ 8. 30163 0.
22806
2027)
2027)
                                 495

-------
      CALCULATIONS f(JK ORAVIMETRIC FLOW  EUPtRIMtNTS




C-70-77  TBfATCO HUH 2« NH4UM
HUN NO. • 198 S02 • 2000. PPM TFMP • 200. DEC. F. 	 r 	
OAII: . ~9 16 'll~ NO • 	 150. "»M FITI '• '" 1500. tC/HIN ~
DRY MT.- 103.10 MC O2 * 3.5 X H2S04 • 77.32 *
CO?R£CTlyN« -5.|0 KG H20 « 6.0 *
K£AN LOAp
GUI S02/100 CMS C
0.95503

	


<
-----
"*

-•

	



0.99421
1.0)094
1.06763 	
1.10686
1.14604
1.18767
1.22665
1.2611)
1.29787 ..
1.33950
1.38113
. ..1.40316 ....
1.42031
1.44969
1.48397
1.52071
1.55499
I.5H977
1.62356
1.65784
1.692J2
1.72641
1.75824
1. 79QOB
1.82681
1.86109
-1.H9Z93.
1.97129
2.09128
2*. 1B6Z9
2.27984
2.37290
2.46350..
2.55411
2.64717
2.74022
2.83328
2.92633
3.01918..
3.10999
3.19815
•• 3.38181
3.47731
1.57787
3.66832
3.76628
a. 86 178
3.95728
4.05523
4.15074
4.24624
4.34664
4.44950
4.57438
4.67479
4.75315
4.90498
5.10823
$.31148
5.51473
5.71790
... 5.91879
6.11714
6.31)05
. 6.50651
6.69996
6.89587
7.0942,
7.29502
7.49583
.. 1.69416 _..
7.89009
8.09579
. B. 30)94
8.49739
8.68595
_ B. 87696... _
9.06797
9.2565)
9.44754
9.63854
9.62466
J0.0107I_ _
10.11076
10.221)1
10.J4070 	
DIFFERENTIAL RATE
MGH S02/CH C-HIN
0.39182
0.39182
0.34287
~~ 0.39182
0.39175
0.44084
0.34280
0.34287
0.39182
0.44077
0.39182
Q..04895
0.29305
0.29)85
	 0.39162 	
0.)42B7
0.34280
0.34280
0.342B7
0. 14780
0.34287
0.29)85
0.391 /•>
0.29)92
0.47345
0.32650
0.31019
0.31019
0.31019
0.79185
0.31019
0.31019
0.51019
0.31016
0.31019
0.11019
0.29387
0.29385
0.11019
0.31019
0.32650
O.V1019
0.32650
0.32650.
0.31019
0.32650
0.32650
0.31019
0.32650
0.34285
0.34285
0.48974
0.17958
0.34285
0.3)468
0.3428)
0.33468
0.3428)
0.33466
	 0... J34.de 	 	
0.32652
0.32650
. £.3.10.15 . .
0.32650
0.32652
. . 	 0.33468 . ..
0.31466
0.3)468
	 0.32650. 	
0.32652
0.35416
... 	 0.33466 	
0.31019
0.31835
0.31835 , ,
0.31815
0.31019
0.31019
0.31019
0.11018
0.08979
0.21224
. „ .D.llZil ..
MEAN LOAD
CMS AC ID/ 100 CMS C
1.46239
1.52238
1.57863
1 .63488
1.69488
1.75487
1.81862
1.87861
1.93111
1.98736
2.05110
2.11485
2.14860
2.17484
2.21984
	 2. 27233. _ 	
2.32858
2.38108
2.4)358
2.48607
2.53857
2.59107
2.64356
2.692)1
2.74106
2.797)0
2.84980
2.89855
3.01854
3.20228
3.49101
3.63350
3.77224
3.91098
4.05347
4.19597
4.33845
4.48094
4.62343
4.76218
4.89716
5.03590
5.17840
5.32464
5.47088
5.61712
5.76711
5.91334
6.05959
6.20957
6.35581
6.50206
6.65580
6.81329
7.00453
7.15827
7.27826
7.51075
7.82198
8.13321
8.44444
8.75566
9.06314
9.36688
9.66686
9.96309
10.259)1
10.55929
	 	 10.6630)
11.17050
11.47798
	 	 .11.78171 	
12.08170
12.39666
	 .12.71541 	
13.0116)
13.300)7
	 13.5928*
13.8853)
14.1 7406
. 	 14.46654
14.74902
15.04401
15.12899
15.51272
15.65147
15.84645
DIFFERENTIAL RATE
MCH AC10/CM C-MIN
0.59997
0.59997
0.52502
0.59997
0.59997"
0.59986
0.67504
0.52491
O. 52502
0.59997
0.67493
0.59997
0.07495
0.44995
0.44995
0.59997
0.52502
0.52491
Q. 52502
0.52491
0.52502
0.52491
0.52502
0.44995
0.52502
0.59986
0.45007
0.52491
0.72497
0.49996
Q.47497
0.47497
0.47497
0.44995
0.47497
0.47497
0.47497
0.47494
0.47497
0.47497
0.44999
0.44995
0.47497
0.47497
0.49996
0.47497
0.49996
0.49996
0.47497
0.49996
0.49996
0.47497
0.49996
0.52498
0.52498
0.74992
0.27498
0.52498
0.51247
0.52496
0.51247
O. 52496
0.51245
0.51247 	
0.49998
0.49996
0.48747
0.49996
0.49998
	 0.5124? 	
0.51245
0.51247
	 0-49996 __
0.49498
O.S4997
0.51245
0.47497
0.48747
0.46747
0.48747
0.47497
0.44996
0.47497
0.4749T
0.47496
0.1)749
0.32499
0.324*1
                              496

-------
                        APPENDIX A-18

           LITERATURE STUDY ON SOLVENT EXTRACTION


 A literature survey on the removal of sulfur from carbon" by
 extraction was made.

 The paper by Prchlik,  et al.14  was of particular interest.
 The paper discussed a detailed study based on both literature
 and experimental work of sulfur extraction from spent gas
 works purification mass (iron oxide).   Literature references
 on 10 solvent systems  for sulfur extraction from spent purifi-
 cation mass were given.  Solubility data for sulfur in various
 solvents were given.  These data are shown in the following
 section.  Diagrams of bench scale extraction apparatus and
 proposed commercial equipment are given.   In reviewing various
 solvents and running bench scale tests,  Prchlik,  et al.  reached
 the following conclusions:

      1)  Carbon disulfide,  while an excellent solvent,  is
          discounted due to the-health  and explosion hazards
          inherent in its  handling.

      2)  Chlorinated solvents,  trichloroethylene  and dichloro-
          benzene, were discounted primarily due to cost
          although it was  also mentioned  that trichloroethylene
          will not remove  the  pitch or  naphthalene present in
          the gas being treated.

      3)  Tetralin was  considered an  excellent solvent but was
          discounted because of  expense and difficulty in
          removing it from the purification mass.

      4)  A toluene-xylene mixture was  considered  the best
          solvent in view  of the  requirement to remove pitch
          and naphthalene  as well  as  sulfur to regenerate the
          purification mass.

Ammonium sulfide was not  considered  by the authors,  presumably
because of its  reactivity with  the iron  oxide.

Equilibrium  Data -  Sulfur-Solvent  Systems

      Solubility of  Sulfur in  Ammonium  Sulfide

No extensive  data on the  solubility  of sulfur in  ammonium
sulfide was  found.   Previous  extraction processes  operated
near  room temperature and under  these  conditions  the solubility
was reported  to be  18-2470 by  weight  of sulfur in  solution14'15.
Since the  pressure  of H2S and NH3 were important  for extraction
studies  at higher temperatures  these data  are shown in
Tables A-1B-1 and A-18-2  and  Figure  A-18-1.

                            497

-------
Table A-18-1.
VAPOR PRESSURES OF H2S, NH3,  AND H20
OVER AQUEOUS (NH4)2S SOLUTIONS
Temp . ,
°C
20
20
20
20
20
40
40
40
40
60
60
60
60
NH3,
% by Wt.
1.38
2.68
6.77
8.05
9.41
2.31
5.88
7.21
9.34
3.22
5.54
6.80
9.00
H2S,
% by Wt.
1.40
2.68
6.81
8.03
9.40
2.33
5.86
7.26
9.36
3.25
5.56
6.81
9.05
Vapor Pressure, mm. Hg
H2S
53.3
65.6
130.1
154 . 8
190.0
92.0
183.4
220.5
293.2
134.1
205.0
250 . 9
365.0
NH3
0
0
0
5.6
13.0
8.2
22.2
26.9
30.4
25.5
48.5
76.1
145.0
H20
16.3
16.2
15.8
15.1
14.3
49.1
44.7
48.4
47.9
125.1
127.3
113.5
105.0
Table A-18-2.
VAPOR PRESSURES OF H2S, NH3,  AND H20
OVER AQUEOUS (NH4)2HS SOLUTIONS
Temp . ,
°C
20
20
NH3,
% by Wt.
0.80
2.14
2.97
H2S,
% by Wt.
1.58
4.23
5.93
Vapor Pressure, mm. Hg
H2S
115.7
163.0
197.6
NH3
0
0
0
H20
13.9
15.2
16.1
                       498

-------
Figure A-18-1.


1000
    Equilibrium vapor pressures of hydrogen
    sulfide and ammonia over aqueous
    ammonia solutions at 20°C
                            Hydrogen Sumde
                                 2.On
                                 l.On
                                 0.5
   0
0.2         0.4        0.6        0.8

        Mole H7S/Mole NH  (R)
             £        O

            499

-------
     Solubility of Sulfur in Carbon Disulfide

The solubility of sulfur in carbon disulfide is strongly
dependent upon temperature, reaching 9070 at 98°C.   Data from
the literature on solubility are contained in Table A-18-3  .
          Table A-18-3.
SOLUBILITY OF SULFUR IN
CARBON DISULFIDE
Temp. ,
°F
-110
-100
-90
-80
-70
-60
-50
-40
-30
-20
-10
% Sulfur
in Solution
1.0
1.5
2.0
2.5
3.2
4.2
5.5
7.1
9.5
12.0
15.0
Temp . ,
°F
0
10
20
30
40
50
60
70
80
90
98
7o Sulfur
in Solution
19.0
23.5
30.0
38.5
50.0
60.0
66.0
71.0
78.5
86.0
90.1
     Solubility of Sulfur in Xylene

The solubility of sulfur in meta and para-xylene is up to
21.8% in solution is shown in Table A-18-416.   There is no
solid phase of sulfur in equilibrium with the solution above
21.8% and a liquid-liquid separation occurred.  There was
                            500

-------
        Table A-18-4.  SOLUBILITY OF SULFUR IN XYLENE


     m-Xylene

          Temp.. °C    % Sulfur in Solution
             25                1.969
             45                3.604
             80               10.29

     Rhombic Sulfur-p-Xylene
          % Sulfur in Solution    Equilibrium Temp. , °C
                  11.0                     85.0
                  13.95                    92.5
                  17.85                   100.5

     Monoclinic Sulfur-p-Xylene
          % Sulfur in Solution    Equilibrium Temp., °C

                  16.25                    98.2
                  16.3                     98.0
                  17.85                   103.3
                  20.38                   106.0
                  21.8                    107.0
apparently the formation of amorphous sulfur.  Table A-18-5
gives the solubility results before measurable amounts of
amorphous sulfur were formed.


These data indicate that sulfur and p-xylene are initially
mixcible in all proportions above about 190°C.  However, if
the equilibrium temperature is maintained, reseparation of
liquid phases occurs, probably due to the formation of
                            501

-------
  Table A-18-5.
SOLUBILITY OF SULFUR IN p-XYLENE ABOVE
21% CONCENTRATIONS BEFORE PHASE
SEPARATION
% Sulfur
in Solution
20.38
21.8
25.9
27.95
28.04
30.22
31.95
34.6
34.9
39.9
44.0
Equilibrium
Temp . , °C
94.0
101.0
117.7
124.5
124.2
130.0
137.3
144.5
149.0
158.5
167.0
% Sulfur
in Solution
44.1
45.7
46.3
48.3
61.7
71.2
81.0
85.6
87.9 .
90.0
91.0
Equilibrium
Temp . , °C
167.5
171.0
175.0
175.0
190.0
190.0
184.0
176.0
162.5
150.0
143.0
amorphous sulfur,  resulting in a rise in the temperature
of complete miscibility.   The equilibrium temperatures
finally obtained are contained in Table A-18-6.
       Table A-18-6.
     SOLUBILITY OF SULFUR IN p-XYLENE
     AT ELEVATED TEMPERATURES
70 Sulfur
in Solution
16.25
21.8
25.9
27.8
27.95
29.1
30.22
31.95
34.6
34.9
36.0
Equilibrium
Temp . , °C
80
109.0
121.7
127.0
129.0
132.0
133.7
141.5
148.25
150.0
154.0
70 Sulfur
in Solution
39.9
44.0
44.1
45.7
46.3
48.3
87.9
90.0
91.0
96.2

Equilibrium
Temp. ,°C
165.0
174.5
174.5
179.5
183.5
196.0
177.0
155.0
147.5
84.0

                          502

-------
The equilibrium temperature rises with  sulfur  concentration
below 48.3/o and decreases with  sulfur concentration  above
87.9/0.  There does not appear to be  a maximum, however.  Rather
the low and high concentration  curves appear to be entirely
separate.  The temperatures above which two phases exist and
below which one phase exists are:
            S in Solution,    Equilibrium Temp.,
                 44.0
                 46.3
                 48.3
                 87.9
                 90.0
                 91.0
        235.0
        220.0
        206.0
        187.0
        203.0
        205.0
Smisek and Cerney17 also present data on the solubility of
sulfur in xylene as shown in Table A-18-7.  These data agree
rather well with the literature information in previous tables
              Table  A-18-7.
SOLUBILITY OF SULFUR
IN XYLENE
Temperature,
°C
25
45
85
100
107
Concentration ,
Wt. %
1.73
3.24
10.78
18.8
24.1
                            503

-------
The following equilibrium data as presented in Prchlik's
article!^ are referenced to the original author:

     System:  Sulfur-Benzene18
Temp . , °
25
54
84
C g. S/100 g. Sat
2.074
5.165
13.02
. Soln.



System: Sulfur -Toluene
Soln.
Temp . ,
OF
-10
0
0
13
15.5
20
23
25
35
40
50
54
60
70
80
83.5
90
100
Dissolved g. of S
in 100 g. of
Sat. Solns .
0.576
0.923
0.897
1.545
1.649
1.827
1.889
2.018
2.722
2.35
3.68
4.85
5.27
7.83
11.1
11.64
15.3
20.9


Determined By
Jacek19
Jacek19
Hildebrand-Jenks 18
Delaplace20
Jacek19
Delaplace20
Delaplace20
Hildebrand-Jenks 18
Hildebrand-Jenks L 8
Burden-Newling 2 !
Burden-Newling
Hildebrand-Jenks 18
Bur den - Newl ing 2 ^
Bur den - Newl ing
Bur den- Newl ing2 ^
Hildebrand-Jenks l 8
Bur den-Newl ing •"•
Bur den - Newl ing 2 1
System: Sulfur-p-Xylene22
Temp . , °
85
92.5
98.0
100.5
107.0
117-121
124-129
C g. S/100 g. Sat.
11.9
13.95
16.3
17.85
21.8
25.9
27.95
Soln.







                            504

-------
Bituminous
Pitch Oil Fraction
Temp . B . P .
°C S.G.
15
30
50
80
100
110
120
130
, °C: 80-100
: .87
2.1
3.0
5.2
11.8
15.2
	
	
	
85-120
.88
2.3
4.0
6.1
13.7
18.7
23.0
27.0
	
120-220
.882
2.5
5.3
8.3
15.2
23.0
26.2
32.0
38.7
i i
Coal)zz
by Boiling Point
150-200
.885
2.6
5.8
8.7
21.0
26.4
31.0
38.0
43.8
210-300
1.01
6.0
8.5
10.0
37.0
52.5
105.0
	
	
Range
220-300
1.02
7.0
8.5
12.0
41.0
54.0
115.0
	
	
505

-------
                        APPENDIX A-19
      DETAILED DATA FROM COMBINED SULFUR STRIPPING/H2S
                     GENERATION STUDIES
                                                        Page

1.  Run SHG-1                                            507

2.  Run SHG-2                                            512

3.  Run SHG-3                                            517

4.  Run SHG-5                                            522

5.  Run SHG-7                                            527

6.  Run SHG-8                                            532

7.  Run SHG-9                                            537

8.  Run SHG-10                                           542

9.  Run SHG-11                                           548
                            506

-------
                        RUN SHG-1
A.  EXPERIMENTAL DATA - IJ2.S GENERATION/S STRIPPING

    1.   Virgin Carbon
        a.  % Sulfur (Combustion Anal.), Psc

    2.   Inlet Carbon -
        a.  %, Sulfur (Combustion Anal.), Psi
        b.  Acid Titration, Pvi
        c.  Material Rate, RI
7.
                                               =  0.65%


                                               =  20.70%

                                               =  40.6 Ibs./hr.
    Intermediate
    a.   Stage 8,
    b.   Stage 7,
        Stage 6,
        Stage 5,
        Stage 4,
        Stage 3,
        Stage'2,
        Stage 1,
        c
        d
        e
        f
        g
        h
Stage Carbon
% Sulfur, PS8
% Sulfur, PS7
% Sulfur, Ps6
% Sulfur, PS5
% Sulfur, PS4
% Sulfur, Ps3
% Sulfur, PS2
% Sulfur,
    Outlet Carbon
    a.   %, Sulfur (Combustion Anal.), Pso
    b.   Material Rate, R0
                        /
    Inlet Gas
    a.   % H2 (26.0% by Rota)
    b.   H2 Gas Rate (55% @ 4.3 PSI)
    c.   N2 Gas Rate (25.8% of 640 @ 4.3 PSI)

    Intermediate Stage Gas Analysis

                      H2S  % N2   % SO2  % H20
                                                      15.79%
                                                      37.3 Ibs./hr.
                                                      26.8 Chrom.  %
                                                      66 CFH @ 70°F
                                                      188 CFH @ 70°F
                                                    % CO   % CO2







1
2
3
*j
4
^r
5
«/
6
\*'
7
Outle
a.
b.
c .
d.
e.
f .

g-
h.
7°
10
01
lo
7
10
7
to

7
lo
7
10
21.4
4.1
21.8
1.3
18.1
16.0
15.8
0
0
2
0
6
6
8
t Gas Analys
H2
H?S
N2
SO?
H20
CO

CO?
Sulfur




(as
.88

.96

.0
.2
.4
is




si)
72
70
71
91
71
71
71






.0
.4
.7
.1
.9
.4
.0





i
0
0.3
0
0
0
0
0






0.08
0.56
0
0
0.14
0.49
0.90

=
—
=

=
0
0
0
0
0
0
0
1 ^
16
4
68
6


1







f^ nt
.27o
1%
.3%
f\ Of
.2/0
.3%
f\m
n i
* \J fo
S7
. ~> lo
0.04
0.05
0.04
0.04
0.04
0.05
0.10






                           507

-------
 8.
        Temperature
          Stage  Carbon/Gas, °F

            1
            2
            3
            4
                                     Stage  Carbon/Gas,°F
                  768/800
                  111/
                  781/800
                  778/
                                  5
                                  6
                                  7
                                  8
801/806
799/
---/801
734/
  9.
        Cyclone Product
        a.   Sulfur                     =
        b.   Material Rate              =
        c.   7o Material +40 Mesh
        d.   % Material -40 Mesh

B.   SULFUR MATERIAL BALANCE,  SULFUR REMOVAL, AND H2S CONVERSION
  1.  Run Start
 3

 4,

 5.

 6.

 7.


 8.

 9.
10.

11.
12.

13.
     Run Times
         Run Time
         Steady State Period
         Inlet Carbon Analysis
         Outlet Carbon Analysis
Inlet Sulfur Loading,
Outlet Sulfur Loading, PSQ

Inlet Material Rale, Rsi
Outlet Material Rate, RSo
Cyclone Sulfur Loading, P
                                           -1680-1690
                                          1680-1890
                                          1720-1890
                                          1647-1817 (-73 tnin)
                                          1776-1946 (+56 rain)

                                          20.70%
                                          15.79%
                                          40.6 Ibs./hr.
                                          37.3 Ibs./hr.
                                 scy
        Cyclone  Material  Rate,  RSCy    =  0.0055 Ibs./hr.
        Gas  Rate In,  qT                =  254 CFH @ 70°F
        N2 Rate  In,  q^2                =  188 CFH @ 70°F
        H2 Cone.  In,  100
        112 Cone.  Out,  100

H2S Cone. Out, 100

S02 Cone. Out, 100 ygo

1120 Cone. Out., 100 (yH2o)o

CO Cone. Out, 100 YcOo
C02 Cone. Out, 100 (vr)
                    " ^

Sulfur Vapor Out, RSVO
                                 O
          negligible
          in balance
                            508

-------
                                               GAS AND CftRBON  rLOW RATES
                                                                                                      j g- - r.?

^—f- -
p _
r
•«=:,-•>, NOTTS'


' ^'°0^' — |
GAS PLOW RAT^^
C, 3£a'_ L^ 3
c-6

»?. --
— | 	 (•
SO'A
P=cs
N2
" "
— fcf 	
^C

iS,

* * . - iT ' ' > ' .J 3 ' »' f r • ~ ' fti '<'4~
•%•:
HiGH H2S
fiR

e c r,
' ; ' !
-; t 1 i
^ :L2 ! ^2 ,:_"! !

- • ^
— -J 	 . —


! i
15 > i J J 3 •*••*• i"f J
.-.-'i c>c»e*t os-3-y j







(

















i
;
rE?y ~? *-^""t '





i


1
f-c 4«j Ft-£r:*t*.
1 1 -••
















j i i ( ; j
1


































i




















i

i





! ! • I


rru




t
i








1
1
i i
1 .



1
1
















1
r





















1



ro^« pcpcRFwrfv
•sc*:
















i i



I






t >
i
i




































: 1

>r««sure at' 6u
1.'2 r lev fcr 1


















































































CFH




















LOW H2S
Rfl












'FK



CO").
CFH





















[
I
















. r£00^ wuri~ArmtKt
TYPE
SKiO NO
SAMPLE N
ever Carbcn Ce&l 1*

f> 	 	











































































HZ
RR

•.S
~5


















APR
























































01 R.







































COZ
HR








































iS.
COR.
, CFH
STEfi^
*R
l









































































OCR-
CC
R*
A-"p
CO.T-
) ;
i i
i

















1














i



'












i
1



i
i




















1
; j

t
























l

!
















EX WJ.'ST
°^r"vr
S'-n
•O^-'C
C-;, :-K r^ri =i---«;
: v L fc "

]
-a/
- • i"
LXCj-lo
i

i -=•: <„: 5 p -.-
- ., " - s ff M - - '

«.C-
I
— *".„-•

i










1
j
i





i












2 C ~ • ' » ! 1 - '„

'';.- •" "• ''-'*. '• ~. f *. _ ^. . i

i ^

1


/"
;• r ' -; r
':.'.'-(„?'* ;
I i
V 	 |*""S ~^ r"1 ' • " '
/-,;. -.-v fc t " rt > t
i ' I I
( i ' i i





1






i


' ' J




1




i














































! *
i










i
1 !




1


l '
1 '
i i
i







1




i








|

1



;

f
'






DATE SH-"| OPERATOR _.


Head at N*2 Hotaceter Outlet; ^gp_. - Gai 'low Rr.te, No Correction;
eg; LTA-iOl - N2 Flow for Upper Carbon S ai Leg,
£.. i"5
^ O
C^r



• Gas /lew r.at« Ccrrc
























1


1

1
!
1
RF*D AND CN^r-Pt-7^^^ j
/t/ ^, ^xixy 7
•
-j^J

Ln
O

-------
GAS  AN/LYSIS
                                                         _.
                                                        RJJs so. ;
                                                        DATE    i/J'.'f
Tisr

f;:*,s.»
OPERATOR NOTES

_» 	 ! 	 T lj 	
	 i ^ - -'.___.

•<•«-
- - *'
1 •;-
""it
fc"*"F,
j/T^Sj
' ?'iJ 5- ^**y fa r • « *
i
r —
•15I1
_i£



!/}*«'










i
i
i
1 i

i







i



1


; i
















CROSS jr









V
o
0
INLET «AS ANALYSIS
so2 coz co
H20

1 C '« TV i? £3 i I/.O
A^
?r.s
i
f
5 0 C-li. 0 i 0 ' ?*.% ll.t i u
* ! O <>;i2 4 ' a i 2? I 7(.| |
0 C s^j" 0 • o :3?.7 -;f. f i>
.





! ' '
j.-^fr
>--i K' vu*J*T' ^*f
1


1 ;
i
i







!




• i


{











j ;

i



i











i

I

!

i



•










) i




i
j



i t ;
j












SEFER'NCES:

vw — — •































i

































CARBON SPECIFICATIONS;

^w

TYPE
' SKiO NO.
SAMPLE 1

^0.

	 EXIT «AS At ALYSIS
H2S

S02
, J.
r%t. <> ' '



CO,
CO
1 . ... .>






3.?f a.ist 0140 | o
f-0% MW >\ 0

t.tb































0-111 O^lt-
OILS > 1
1



I
1






























.
















































rt. 0
*, '



*" t 7
', f?

iS-'a.









i

^
A/.
**.

INTERMEDIATE 9AS
STAGE

x i i «


i
3.1
— ~
J.
' *7
;_5
f ?-0
t9-^ (,
t.a/UI.7. '
4-5 ' tli


| ;


1













i
j ;


1



















































1












1


]
L 	 I 	 ,




' i '


1
£
3
V
5
Q>
7
HS





* ~


? .'
-7
^ ?








^ — _<
^
n
& c
v x

j
! i 1
so2 ,co2 ; co
! , i





i
' ' \
o 5?- 3 0 '
(.}<> v-.;rr o i
C ' 5=3' 0 ,
O C SIZ Q '
o 9c-S' o :
£> i O ! 0.{gO' 0 -

' O.;3
ANALYSIS '









>9j
0*^
O
—f
_£_/£
(JT"'
0<-,0
i 1
i !
i
i !


1 |
: i

i


31 p. 7^. r
••- r -. v

i I.A :«'./
'•Z3-1 7.'.?
::^.i."Ti i
';;.;> .-(.o










1 i , •' i ;













i i
i
!


i
•
i
i . ^- i
" • ' •




i ;
j i

i . i ' :















1
: (
1 :
i
j. . . . . 	 i
j (





, '
! 1
! ;
1
I !
i
i



i t
j
)
i '• ' •
'•!',:•
: i
I j : •''••'•: ' :
\ j ; 1 i j
! ! 1 : 1 I'll







': \
\ j
! i
i 1 1 '




! :



1
I J
1
t
i
i

• •

i
i
; i i : i : !



i : !
! ' i
DATE \5~
CT
i S-4
j ^_ y
! 12-8



OPERATOR





1 :




,
! j
1
i ;

- 	 	 -. —
p^^n aND UNCCSSTOOD



4/X. fa

/^/ / k/xiy?}



-------
4"D!A REGENERATOR
                ~~

i~>ie> ' fj^o
TIME
^-^
C*E»ATCR NOTES


COLUMN TEMPERATURES. PRESSURES, AND PRESSURE









COLUMN PRCSSL'RES A«0 PRESSURE DROPS. IN. H_O 1 COLUMN
PI
2
id,: 5 c«t£»» pfti OH
i < -.-^ OH
" -5 '-K^ 1 - X-
r~-j \Z'^-.:e>
•

3


STA
i i
i
• 1
'3 Sis-
/ C '- --i
3
! i
3i
« i
i
A\C
3 i
;
!_;_
6
j
M
M3c
7 JB
|
1
R
9 i
t
; ' ' ' : ' !
/ 7'
i
- / /
ITT — 5"^[^6£ " \tt ' 10 l — — nr*
1
1





i
i

i
f

\ '












l









i








i
i



t



i













I }
;

i i
i





















<



3 2, - y 5 j
• jj < C

1
1
1














'
^ /i
:
iO

Jc-

3 e ,

i 3
* *


_- < .
:
^y^
1
- 6- 1

5-4!


/° ;

f 7
/?

* i • j







i







!
l





























j ; i ,


t

i
1




i







i

I





1










I

i












1


/Q

/O
to
























t .
h;





Tl
42
1

S-'J
7--.'
?,<
.2
_Z
.2

43


44 -35
!



*J5'
l '


DROPS




RUN NO _•? .1 C. . 1
FEED so. - as
DATE 1/31/73

TENPE3ATUSES. -F "T -*^-


49



•37

FFY-VA[ rnNT^O1. i rps T£ *• -^~- F?
T-C WTA <-r= s.£T
•45]<3i «( i-C.O 1:01 -^7. £•.&•*••*'• -•*•

| i ! ; : :

;??i-

i ]
•









j
1
. 1
i










I
i

i

t
r

i

(





t
! i













i





i




i









1
! i
i




i I !






i






j
1




















1 i
i
; t

1

1






i


!
L ^ 	 1 	 .
i


i















i








































'

































*






i





























C=^SS R^FEPFNCES: CARBON SPECIFICATIONS.'
TYPE
SK;DNO
1 SAMPLE


JTA...1 - 1 - **^ TT>'.a^ M OiiLUt if C4li^; IT* J^ - T^c-
NO

r»ltf* *l Cwkce C«.*r Lt

.t.



t are?


.,_.„.




>*7 7^_ f- . ,if A


£/O
SVC
"rcT
SI

tv
i :ll:!
! ! i 1 I
2c-''?2££73 fi5£& ??:? 72 5"
.'.-.ir^;'^ i ur/>i_..^---" -r:--s_j

; i ! ' ' i
j i
j ,





























1
! l ' , i . ! •
i : ' i



1 i !
iii;
: • i i !
! ' • i

]
: ' i



1 i ! ' ;
! ' 1 i




1



!






























1 i i I
I 1 ' t
i ; i i i
1 I '
ill'
1 '• \
1 1 j
i l ! •;! i
i [ ! i 1 l

i

i i
! ! !


,
1


i i
I


i












I |

i |
i '



• i ! i
: ! i !
! 1 i i








i

i
ii i :
i ' i
i • i i
i i * : . ;
; i i i
! : | >

• l .
i !




' 1
; : |
I '












1
! ' 1 !










(
1
' i
	 ^ __ — j.
; ; i








i i i i ;
i
il 1
l
.
l
! 1 i

: 'li- i



1 1
DATE

SHiFTl CPERATCR
8 ~ *t '
4-!2 •
\2-6 1





1



i 1 '
1 ! • ;
t
i i
	 i 	 1 	 . 	 j 	 	 	 . 	 -
i 	 -j
RTAD AND l:N~|—'~TCOD f
— f- ,~f — -£ 	 i
i I

-------
                            RUN SHG-2


A•   EXPERIMENTAL DATA - H2S GENERATION/S STRIPPING

    1.   Virgin Carbon
        a.  % Sulfur (Combustion Anal.), PSC       =

    2.   Inlet Carbon - Precursor C-72-108 - Act.  (0.598)(10~3)
        a.  % Sulfur (Combustion Anal.), Psi       =  20.31%
        b.  Acid Titration, Pv£                    -
        c.  Material Rate, Ri                      =35.1  Ibs./hr

    3.   Intermediate Stage Carbon
        a.  Stage 8, % Sulfur, Ps3
b.
c .
d.
e .
f.
g-
h.
Stage
Stage-
Stage
Stage
Stage
Stage
Stage
7,
6,
5,
4,
3,
2,
1,
7
/o
7
/o
7
/o
7
/o
7
/o
7
/o
7
/o
Sulfur,
Sulfur,
Sulfur,
Sulfur,
Sulfur,
Sulfur,
Sulfur,
PS7
PS 6
PS 5
PS4
PS3
PS2
PSI
    4.   Outlet Carbon
        a.   % Sulfur (Combustion Anal.), Pso       =   4.85%
        b.   Material Rate,  Ro                      =29.1 Ibs./hr.

    5.   Inlet Gas
        a.   % H2 (29.3% by Rotameter)              =  32.0 Chrom. %
        b.   H2 Gas  Rate (57 RRx1.1 FF =   3 PSI)  =  67 CFH @  70°F
        c.   N2 Gas  Rate (41% of 360 @ 3 PSI)       -  162 CFH @ 70°F

    6.   Intermediate Stage  Gas Analysis

          Stage  %  H2   %Jt2_S  % N2   % SO2  % H20  % CO   % CQ2


                                       0.1   0.52     0    0
                                       00        00
                                       0     0.25     0    0
                                       00        00
                                       0     0.41     0    0.05
                                       0     0.61     0    0.1

    7.
                                                      10.0%

                                                      6S'.570

                                                       8.5%
                                                       0
                                                       1.25%
                                                       5.5%
                              512






1
2
3
4
5
6
7
Outle
a .
b.
c .
d.
e .
f .
g-
h.
/o
%
%
to
7
/o
%
%
%






t Ga
"2
H?.S
N2
SOy
H20
CO
C02
7.
24.
24.
21.
13.
10.
8
7
2
5
0
3
s Analy







Sulfur







(as
0
0
1.
4.
6.
16.
sis







-

0
4
1
9








73.3
72.8
74.3
74.6
71.2
73.3








SD

-------
8.   Temperature
      Stage  Carbon/Gas, OF
        1        942/997
        2        970/
        3        982/997
        4        967/

9.   Cyclone Product
    a.  Sulfur
    b.  Material Rate
    c.  % Material +40  Mesh
    d.  % Material -40  Mesh
                                       Stage  Carbon/Gas,°F
                                         5
                                         6
                                         7
                                         8
                                        1001/997
                                         970/
                                         —7970
                                         840/
                                       =  3131  (Start
B •   SULFUR MATERIAL BALANCE, SULFUR REMOVAL, AND H2S CONVERSION

    1
 3


 4

 5

 6


 7


 8

 9

10

11
12

13
Run Start

Run Times
a.   Run Time
b.   Steady State Period
c.   Inlet Carbon Analysis
d.   Outlet Carbon Analysis

Inlet Sulfur Loading, Psi
Outlet Sulfur Loading, PSo

Inlet Material Rate, Rsi
Outlet Material Rate, RSO
Cyclone Sulfur Loading, P
                                       3131  (Started C  at
                                             Feeder +95 min)
                                       3226-3408
                                       3262-3408
                                       3167-3313
                                       3326-3472

                                       20 . 31%
                                       4.85%
                                       35.1  Ibs./hr.
                                       29.1  Ibs./hr.
                                                     (+36)
                                                     (-95)+36
                                                     (+64)+36
                                 scy
                                                %
                                                 °
                                                ;./hrj
Cyclone Material Rate, Rscy    =   0.0033  Ibs

                               =   162  CFH @ 70°F

                               =   32.0 vol. %
                                                       negligible
        Gas Rate In,
        N2 Rate In,
        H2 Cone. In, 100
        H2 Cone. Out, 100
               100
              Out,

              Out,  100 yso

              Out,  100

             Out,  100
              Out,  100
        H2S Cone

        S02 Cone

        1120 Cone

        CO Cone.
        C02 Cone

        Sulfur Vapor Out, RSvo
                               513

-------
             Ss
                      33 ai-
                                                      GAS  AND CARBON FLOW RATES
                                 TYP£
                                        NO.
H',tt.  Pr^ss.
De.-jsit;/;   3-5
 - Prccsure at Outlet, cf ?.ol&=eter Read at N2 Hotaacter Outlet;   App. - Ga.-. F.'ov
6 - K2 Ficv for Lever Carton Seal Leg;   LTA-101 - Ng Flow for Upper Carbon Se> 1 :
C4TE |c
!
> FP? 7? I
it-e, l«o Correction;


*?-Pi£N3..;8?.,fVN
Cor^ - Gas Flow Pate Correct*
RSAD AND UN7r^STOO'D !
^ x. A4J / ii/vb !
i i


-------
                                                                    GAS  ANALYSIS
                                                                                                                               4" OIA. REGENERATOR
                                                                                                                               RUN  NO. S^g- 2.
                                                                                                                               PEED
                                                                                                                               DATE
 T!-
                                                                                                                                 AN")

-------
                                                                                                                                                       4" ;:A RE"EN'-°A'OR
Ul
                                                                                                                                                       RUN NO  .THJSL-Z.-

T'ME O^ERiTGX MOTES
r.-.;--.





V-UI_UIVIIN i trvirtrcA i UKC.O. rK:a

CO'USN Purs?!jR
PI ! ST;G;L
z
L*-'?v. STA?T ^Ar//^
! '=c .M
'*-- C-JL !' £•• »J
"««t ' :\ S
""• '; S
s
•TO

• 7
',
| ,
2 1 3
4
/ccO c^
ES AND PRESS'JP
ANO D^l ri^Vb!
5

! "-' =i II. S ji-u \.S
S
7

I0j2.i
a

	
E DROPS. IN. H-O
:R
9



11



"•"-,•. \-S II.T f \ ? -10 ^ s i s -q
.* ' ^ \ : ' '.5 \-^ .1.9 -i o!: ia-u
(•-iw. • o f\ ' ' i '

t^j, | i ,
£c'^ -"5rC.~ J -^f- -_tJ f ^-y-
!> = ?' <; 7

'.;•• '/.5
1- ^
?2-
-pr-
*v»*-i-!?.t- uc«^tj
i / i
' ' * ( C
	 ^yl ->-.' ,^m°..x £ ,,£ «-*£.
yj*i- f .-f^£Z —t1- cr.-mu. *£•«»••*_ "*• t
7-*^ / * /'«
/ j^gp ^J/
"X
r^ ' c-~ • !
?. « :< • i ; \
i'?

' '
*. & — -
t r p
i-T 1-8
1 &it-O
!

Ut>J 3-' 1^.
i
v/'TH
...
fc*7vfcj?5i,t.'^> VCC'
I'M'?
i ;/o~'/.^


1 I-*
I S J/-7

/ Tit^
2,^,-r' -.-^BJ- ».F*7v/i/5 'ct-.r> ^^(r-3 i
* u*c*
i






i







































!









i
.






!



1 i










1



r.9055 REFERENCES;
•1BD
II^HtllVilVi^i'^*-1
1 ftZ - C,:**?:•„'•* a* •-••e --c f.'.'-i: •-:: c":.-<-~.l ' i
;
i
kn qp
1 ! : ! • ! i • i ill 1
1 • • i i i 1 i i
0 aog.rn',To:~p<: 1i« 'i5« cii |»i» rc"C> -!«•—•- ;?•>! "rf ire' 1 «>•»»' 'to i ' ' <"»a
J 1
s icftrr
V.
t.o| | ^'^
S-4!


5
^,

^























. —












i
l»:-.


'.:



1

at(j/j
— ^
r

1 ! i ! • ! - 1 !i i i
I : i . • • i iii • i '
?Jo I'll ;?'"! »7"'/r'- 7' -J5" .^tr '?>: ''~o ••»:'?:'-' «•<•.-. ' «-"^"c7^i ! '/j?7
y^-^rn 	 i 	 rj— 	 V— ! 	 77-^ 	 J7-U- 	 i 	 j 	 ^ 	 1 	 ! 	 i 	

J ! .
'ft-. i??o We •?/•!.'
~7
(








F*-"
^






i












1





















•raturvi.
L'zjf.a.j&i
•V7o ni5 :*y1o






























1 • • . • 1 ! ! i :
1 i 1 1 , i . - 1 jli';!

fcf&'iTf £Vc'f7o ff> {c-s/se*1;?* •&'-,-: '.r- T/:'- ' HV i--" ' ' ' "VJo
?9"'?A2J S5J /a,-r'-H- .r~J./c«>";«j !f.o "•."•?•:- 'W1 1 ?5>' ^^ '' ' i •=• ^^ I
(iiitaMi ISSP-IcSJ'?'!-''^ ^c 'Sw :?r Emit.

-------
                            RUN  SHG-3


A.  EXPERIMENTAL DATA - H2S GENERATION/S STRIPPING

    1.  Virgin Carbon
        a.  7o Sulfur (Combustion Anal.), PSC

    2.  Inlet Carbon -
        a.  7. Sulfur (Combustion Anal.), Psi       =   20.35%
        b.  Acid Titration, Pv±                    =
        c.  Material Rate, R±                      =30.9  Ibs./hr.

    3.  Intermediate Stage Carbon
        a.  Stage 8, 7. Sulfur, Ps8
b. Stage 7, 70 Sulfur, PS 7
c. Stage 6, 7o Sulfur, P$6
d. Stage 5, 7» Sulfur, PSS
e. Stage 4, 7. Sulfur, PS4
f. Stage 3, 7> Sulfur, Ps3 =
g. Stage 2, 7o Sulfur, Ps2
h. Stage 1, 7. Sulfur, PSI
4. Outlet Carbon
a. 7o Sulfur (Combustion Anal.), Pso = 2.8270
b. Material Rate, Ro =23.85 Ibs./hr.
5. Inlet Gas
a 70 H2 (27.2% by Rotameter) = 29.870
b H2 Gas Rate (4570 Scale, Assume 1.1 PSI) = 52 CFH @ 70°F
c. N2 Gas Rate -