WATER POLLUTION CONTROL
  OIL AND HAZARDOUS MATERIALS PROGRAM SERIES  OHM 72 os 002
       Regulations,  Practices and  Plans  for
         the Prevention  of Spills of  Oil and
             Hazardous Polluting Substances
                                      VOLUME  I
ENVIRONMENTAL PROTECTION AGENCY
OFFICE OF WATER PROGRAMS

-------
    REGULATIONS, PRACTICES AND PLANS
FOR THE  PREVENTION OF  SPILLS OF OIL AND
     HAZARDOUS POLLUTING SUBSTANCES
                VOLUME  I
              October  1971
               Prepared By

             A. E. Wechsler
              J. I. Stevens
               P. A. Huska

        Arthur D, Little, Inc.
    Cambridge, Massachusetts  02140
       Under Contract 14-12-950


                   for


Division  of Oil and Hazardous Materials
       Office of Water Programs

    Environmental Protection Agency
For sale by the Superintendent ol Documents, U.S. Government Printing Office
            Washington, O.C. 20402 - Price $1.75

-------
              EPA Review Notice
This report has been reviewed by the Office of
Water Programs, EPA, and approved for publication.
Approval does not signify that the contents
necessarily reflect the views and policies of
the Environmental Protection Agency, nor does
mention of trade names or commercial products
constitute endorsement or recommendation for
use.
                       ii

-------
                                FOREWORD
     The enactment of the Water Quality Improvement Act of 1970 provided
the necessary legislative force required to set in motion a vehicle
designed to eliminate accicle'nti&JL spiels of -oil and. hazardous materials
through prevention.  This study waif designed to provide a basic working
knowledge and understanding of existing rules and regulations, design con-
cepts and operating practices in spill prevention to satisfy basic require-
ments set forth in Section ll(j)(l)(C) and 12(G) of the Act.

     The main elements of this study are intended to complement an earlier
study entitled, "Spill Prevention Techniques for Hazardous Polluting
Substances" under EPA Contract 14-12-927 and published by the Water
Quality Office, February 1971.  This related report, "Regulations, Practices
and Plans for the Prevention of Spills of Oil and Hazardous Polluting
Substances," Volumes I and II, represents the results of a three-phase study
effort to:  (1) review Federal, State, local, commercial and industrial rules,
regulations, standards and recommended practices to prevent the spills of oil
and hazardous polluting substances, (2) survey selected facilities and plants
in the field to document the state of the art in spill prevention technology
and critically evaluate the "cause and effect" relationship of spill preven-
tion technology to rules, regulations, and standards, (3) prepare a program
plan (prototype plan) that proposes a balanced Federal, State, local and
industry spill prevention program.  Volume I presents the results of Phases 1
and 2; Volume II gives a summary of the program and presents the program plan.

     In addition, this study shows that spill prevention for oil and hazardous
polluting substances is practiced mainly as a result of fire and safety codes.
There are,  in fact, very few spill prevention programs for environmental
protection  at the Federal, State and local levels of government.  The data
documented  in this study and the prototype plan could be used as a basis for
identifying problems associated with spill prevention.

     It is  hoped that this will provide the necessary direction and guidance
for all levels of government and industry to proceed with the development and
implementation of a balanced spill prevention program.
                            H. D. Van Cleave
                            Project Officer
                  Division of Oil & Hazardous Materials
                        Office of Water Programs
                     Environmental Protection Agency
                                   iii

-------
                           TABLE OF CONTENTS

                                                                    Page

List of Tables                                                       vi

I.     SUMMARY                                                        1

II.    INTRODUCTION                                                   9

       A.  Background                                                 9
       B.  The Spill Prevention Problem                              10
       C.  Approach                                                  12

III.   LAWS AND REGULATIONS  FOR SPILL  PREVENTION                     17

       A.  Federal Regulatory  Practice                              17
       B.  State  and Regional  Regulatory  Literature                  22
       C.  Fire Laws and  Fire  Prevention  and Underwriter Codes       30

IV.    TECHNICAL  AND TRADE LITERATURE                                31

       A.  Causes of Spills                                          31
       B.  Equipment,  Design Criteria  and Procedures
              for  Spill Prevention                                    35
       C.  Industrial  Utilization  of Spill Prevention
              and  Control  Techniques                                  47

V.     FIELD  SURVEY                                                  49

       A.  Methodology                                              49
       B.  Survey Results                                           51
       C.  Comparison  with Other  Surveys                             68

VI.    ACKNOWLEDGMENTS                                              73

VII.   REFERENCES                                                   75

VIII.  APPENDICES                                                   77
                                     v

-------
                        LIST OF TABLES

No.

 1     Matrix for Contrasting and Ranking the Main
       Functions or Areas in Liquid Handling Facilities           13

 2     United States Geological Survey—Outer Continental
       Shelf Regulations                                          21

 3     Types of State Water Pollution Regulations                 23

 4     Specific State Spill Prevention, Rules, Regulations
       and Laws                                                   24

 5     Sources Used in Literature Survey                          32

 6     Types, Causes and Remedies for Chemical Spills             33

 7     Types, Causes and Remedies for Oil Spills                  36

 8     Hazard Factors in Chemical Plants                          37

 9     Professional Groups Establishing Equipment and
       Fabrication Standards Pertinent to Spill Prevention      .  40

 10     Typical Publications on Handling Flammable and
       Hazardous Materials                                        41

 11     Case  Study Examples of Procedures for Overcoming
       Oil Pollution                                       "       43

 12     Typical Check List for Process Examination                 44

 13     Check List for Heater, Common Transport and
       Storage Operations                                         46

 14     Facilities, Agencies and Organizations Visited  in  ,
       Field Survey                                               50

 15     Summary of Spill Prevention  Practices
       in Storage Areas                                  -53

 16    Summary of Spill Prevention  Practices
       in Transfer Areas                                          57

 17    Summary of Spill Prevention  Practices Used
       in Loading and Unloading Areas                             50

 18     Summary of Spill Prevention  Practices Used  in
       Process Areas                                              53

 19     Waste Treatment Practices Which Aid  Pnin
       prevention                              *                   /--^

 20     Summary of Spill Prevention  and Control
       Practices at 107 Facilities                                70

                              vi

-------
                              I.   SUMMARY
PURPOSE AND SCOPE
      The purpose of this program was to assess the state of  the art of
technology for the prevention, detection and control of spills of oil and
other hazardous materials.  More specifically, the goals were to:

      •  review and analyze "fail-safe" practices—regulations,
         design concepts and  criteria, equipment and operational
         procedures used to prevent, detect or control spills or
         leaks of oil  and hazardous materials;
      •  determine the level  of utilization of these practices in
         industrial facilities and distribution systems;
      •  prepare a prototype  plan for use  in developing federal,
         state and local regulations, policies and programs pertain-
         ing  to the prevention, detection  and control of spills of
         oil  and hazardous materials.

      We focused attention on prevention of accidental spills because pre-
vention is the first  line of  defense against environmental damage and
strongly influences the requirements for detection and control.  Emphasis
was  placed on methods  for preventing spills of oil, other hydrocarbons
and  hazardous chemicals at refineries, terminals, storage, distribution,
petrochemical,  rubber, plastics, chemical and metal products facilities.
Prevention, detection  and control practices in off-shore and  on-shore oil
production were given  only limited study because of their rather special-
ized technology.
 APPROACH
       To accomplish the program objectives,  we  undertook three  tasks:
 (1)  a literature survey, (2)  a field survey  of  industrial facilities  com-
 bined with discussions with industrial environmental managers and  staff
 members of federal, state,  and local regulatory agencies as  well as
 designers/architects/engineers of industrial facilities, and (3) an analysis
 of the information gained and synthesis of a prototype plan.

       We reviewed the laws, regulations and  operating orders of federal
 agencies, such as the Environmental Protection  Agency, Department  of
 Transportation, Department  of Interior, Corps of Engineers;  the environ-
 mental and health agencies  of about 40 states;  and several metropolitan
 districts.  We reviewed the recent technical literature, concentrating on
 those journals which represent the petroleum and chemical industries  and
 environmental and waste treatment technologies.  We reviewed the publica-
 tions of trade, safety, fire protection and  insurance associations,  and

-------
examined industry and government agency reports of spills.  We also
examined a cross section of manufacturers' literature on spill prevention,
detection and control.

      Our field surveys were conducted in four geographic locations:
Houston, Texas; California; the New York-New Jersey metropolitan area; and
the Illinois-Michigan area.  We visited 23 operating facilities representing
petroleum refineries, bulk storage and distribution, petrochemical, chemical,
synthetic rubber, plastics and metal products industries to determine^the
level of spill prevention currently practiced.  Many of those facilities
combined refineries, terminals, or several types of chemical processing and
materials handling methods.  We discussed the present use of prevention,
detection and control techniques, procedures and equipment with plant
managers and pollution control staff, and requested information on future
needs of industry.  We discussed regulatory practice and the state of the
art of prevention during visits with eight state, federal and/or local
regulatory agencies.  We visited five architect-engineering firms res-
ponsible for the design and construction of new industrial facilities to
determine the spill prevention measures which they presently incorporate
in new facilities.

      We examined and analysed the information derived from the litera-
ture  and field visits, and summarized the prevention technology applicable
to five major "unit operations" encountered in industrial facilities—
storage, transport, loading and unloading, processing, and waste treatment
of oil and hazardous polluting materials.  We compared our results with
previous surveys at different locations.  From this state-of-the-art  summary,
we developed a prototype plan which considers possible spill prevention
regulations, penalties and incentives; development of an integrated pre-
vention program; educational programs; and future equipment needs for
prevention, detection and control.
 RESULTS AND CONCLUSIONS
 Regulatory Literature

       •  Present federal regulations  are directed  at  establishing water
          quality and prohibiting spills  of  oil  into the  public  waterways;
       •  The federal government  has the  mandate to study,  encourage,  and
          establish methods for prevention of  spills,  but,  with  a few
          exceptions, existing regulations provide  little guidance or
          detailed information on prevention practices.
       •  The prevention of spills during offshore  oil production is
          specifically addressed  by the Department  of  Interior,  U.S.
          Geological Survey Operating  Orders in  which  detailed prevention
          practices are described.

-------
      •  The water quality regulations of the states vary considerably
         in scope and content:  emphasis is placed on water quality
         standards and municipal treatment programs, not on industrial
         waste treatment.

      A majority of the states have regulations which provide for issuing
permits, determining compliance and revoking permits for both municipal
and industrial waste treatment facilities; one third of the states have
specific regulations pertaining to prevention spills of oil; less than
half of these also address spills of hazardous polluting materials.

      •  The major oil production states have specific .regulations con-
         cerning the prevention of oil spills during production and
         transport to processing facilities.
      •  Several states have  recognized the potential for pollution by
         oil and hazardous materials during transport and at terminal
         operations and have  provided guidelines or detailed specific
         spill prevention procedures.

Trade and Technical Literature

      * The principal causes of spills of oil and hazardous materials
         during fluid handling are human error, operational failures and
         equipment failures.
      •  Most of the technical literature on spill prevention is directed
         at the prevention of hazards to personnel and property by fire,
         explosion and toxic  effects—protection of the environment is
         discussed infrequently.
      •  Industrial codes and standards adequately address problems of
         fire and design of equipment against mechanical failures; spill
         prevention is not specifically addressed, but most of the
         practices described  in these codes and standards are valuable
         adjuncts to spill prevention.
      •  Although complete descriptive literature data on "fail-safe"
         equipment for spill  prevention and instrumentation for spill
         detection is sparse, the trade literature of manufacturers
         indicate that an adequate number of devices are commercially
         available.

Field  ^urvey

General Observations

      •  The most sophisticated prevention, detection and control tech-
         nology is applied to those substances most hazardous to people,
         most damaging to property, or of high commercial value.
      •  The best developed containment, monitoring and treatment facili-
         ties are usually installed at facilities where the consequence
         of uncontrolled spills and leaks would be immediately evident
         through such visual  indicators as floating substances, massive

-------
        fish kills, etc.  The major attention has been given to oil,
        because it is the largest volume handled in commerce and is
        easily detected when spilled.                     _  _           _
        Highly automated processing plants may have a significant poten
        tial for spills or leaks of hazardous polluting substances
        because the reduced number of operating personnel does not permit
        visual observations throughout the facility and because even the
        most sophisticated control systems are incapable of detecting
        small leaks and spills which can be extremely hazardous if
        allowed to enter the water.
        Very little instrumentation is installed solely for the detection
        of spilled substances; process instrumentation used in the trans
        fer, storage and processing of hazardous polluting substances is
        applicable to detecting large spills but of doubtful value in
        detecting spills such as from small leaks.
        Catastrophic occurrences with a high potential for large volume
        spills, such as a tank rupture, receive the most public^atten-
        tion and consequently greatest consideration of prevention;
        chronic leaks and small spills which enter water probably have
        a greater accumulative effect but are given less attention at
        facilities.
        Separating areas of high spill potential and using collecting
        sewers and ditches that lead to containment areas where spilled
        substances can  be monitored, treated and recovered is the most
        effective means of preventing hazardous polluting substances from
        entering water  courses.
        Passive barriers for preventing the flow of spilled liquids are
        a highly desirable method  of containment; however, containment
        dikes  surrounding liquid storage  tanks can often be breached or
        overflowed when a catastrophic failure occurs.
        Little consideration has been given to the possibility of  ground
        water  pollution as the result of  leaks and spills; however,
        designs  of modern facilities are  giving  this more consideration.
        Wide  variations exist  in the maintenance, housekeeping and opera-
         tional practices of  facilities handling  similar types and  volumes
         of  hazardous  polluting substances; therefore there is a broad
         range  of  spill  incidences  and prevention measures.
Causes of Spills
         Facility operators consider poor housekeeping practices and
         failure of operating personnel  to perform their assigned jobs
         to be the principal causes  of spills.
         Although equipment failures are known  and documented causes of
         spills, they are probably less  significant and more easily
         corrected and prevented than failures  of operating personnel to
         perform satisfactorily.

-------
      •  The  potential for spills of hazardous polluting substances
         increases when facilities are being renovated or when repairs
         are  being made.
      •  Loading and unloading operations have the highest spill potential
         because of the temporary nature of the connections between trans-
         port vehicles and transfer equipment and the large volumes of
         fluids transferred.   The weakest points in transfer systems (pipe-
         lines) are at connectors, flanges, joints, valves, pumps and
         instrumentation inlets.
      •  Operating personnel generally have little awareness of the poten-
         tial hazardousness of many substances when introduced into the
         water environment. ' Little attention has been given to the role
         of some actions, such as fire fighting in transporting spilled
         substances into water courses.

Specific Prevention Practices Used

      The following specific prevention, detection, and control practices
were observed most often in this field survey.
Practice

Dikes, fire walls or barriers around
tanks
Monitoring of waste system effluent
to aid in spill detection
Hard surfaces or surfaces sloped and
graded toward ditches or drainage
system
Curbing, gutters or drainage ditches
around tanks or areas

Separate process and storm water
sewers

Holding or diversion ponds or
lagoons
Specific procedure for diverting
or treating initial rainfall
Periodic inspection of all pipe-
lines for leaks, combined with
preventive maintenance
All pipelines located above
grade to facilitate inspection
Collection sumps and oil separators
at each area
Manual gauging of tanks at regular
intervals
Swivel joint loading arms or rigid
connectors
Area

Storage

Waste treatment

Process
Loading and unloading
Storage
Loading and unloading
Process
Storage
Waste treatment
Process
Storage
Waste treatment

Waste treatment

Transfer


Transfer

Loading and unloading
Process
Storage

Loading and unloading
Observed at
    % of
 Facilities

     91

     52

     52
     30
     30
     48
     48
     30
     48
     30
     26
     43

     35

     35
     35

     35
     26
     30

     30

-------
      Several of the facilities visited have established management practices
to aid spill prevention.  These included:  employee motivation programs,
placing responsibility for spills on individual operators, pollution contro
education programs, spill emergency reporting and specific training pro-
grams emphasizing pollution control.

      In comparing the results of the present survey to similar surveys
at other locations, we found the following prevention practices most
commonly used:

                                      % UTILIZATION OF PREVENTION PRACTICES	
                                   This     	rnrnpnsite Survey	,.
Practices                         Survey    Chemical Facilities Total Facilities
          (Number of Facilities)     (23)	(31)       	LLSLD	

Complete Diked  Storage              52               42                44
Tank Level Alarms                    9               16                 8
Above Ground Transfer Lines         35               23                H
Curbed Process  Areas                48               52                22
Process Area Catch Basins           26               16                13
Holding Lagoons                     43               42                17
Primary Waste Treatment             52               55                31
Secondary Waste Treatment            9               16                 6
Spill Cleanup Equipment             13                3                16
Preventive Maintenance Program      35               33                18
Spill Control Plan                  60               6.1                39


Prototype Plan

      The prototype plan  (Volume II) consists of a series of recommended
actions  to  raise  the  level  of spill prevention- throughout government and
industry.   Some of the most important recommendations are:

      •   Oil  and  hazardous  polluting substances should be placed on the
          same  federal regulatory basis  in  terms of spill definition, pro-
          hibiting spills, spill prevention measures, penalties and
          incentives.
       •   States should be encouraged to evaluate, standardize  and  expand
          their  regulations  and procedures  for prevention of  oil spills  as
          well  as  other hazardous materials to be commensurate  with
          federal  regulations.
       •   Facility operators should be required, as part of their waste
          discharge permit applications,  to submit plans for  preventing
          and  controlling spills in  accordance with federal and state
          regulations.
       •   Existing codes and regulations covering fire  protection,  pressure
          vessels,  and pipelines should  be  expanded to  include  provisions
          for  the  prevention of spills of oil and hazardous materials.

-------
Fire, safety, building, and air pollution regulatory groups
should be encouraged to assist in water pollution prevention.
An educational program on spill prevention, detection and control
using several levels of communication media should be instituted
by  government and industry—specific emphasis should be placed
on the individual's contributions to prevention, and in placing
environmental protection at the same level as safety.
Government and industry should cooperatively conduct demonstra-
tions of integrated spill prevention programs designed to
develop the required methodology and data and to show how best
to implement spill prevention.  These programs should include:
assessment of hazards; establishment of short and long range
levels of spill prevention; evaluation of existing prevention,
detection and control technology; development and implementation
of additional required prevention measures; establishment of a
continuous program of quality control for spill prevention;
documentation and evaluation of the effectiveness of the program.

-------
                            II.   INTRODUCTION
A.   BACKGROUND
    During the past several years, concern over water quality has been
strongly aroused by major pollution incidents and by a growing awareness
of the insidious environmental effects of the smaller leaks and spills
of oil and other hazardous materials  that occur daily on the land and in
the water.

    In response to this  concern, government, industry and public groups
have proposed and conducted a number  of programs aimed at controlling
spills of hazardous materials and at  cleanup or recovery procedures.
The Environmental Protection Agency,  the U. S. Coast Guard and some state
agencies are conducting  broad programs to develop methods and equipment
that will eliminate or confine hazardous materials should these be re-
leased into the water.   The petroleum companies, both individually and
collectively, are developing methods  of cleaning oil from the water.
Other industrial organizations have sought means to identify spills,
control them, and clean  them up.  Public interest groups have contributed
through their exposition of environmental damage and their attempts to
assure passage of pollution control legislation.

    Unfortunately, few of these  efforts have been directed at the most
promising solution to the problem—stopping pollution at the source
through adequate spill prevention measures.  Prevention makes both
economic and environmental sense.  Cleaning up the pollutant during the
Santa Barbara incident,  for example,  may have cost as much as $5 million.
In  the recent Shell fire, pollution and well damage reportedly added up
to  more than $15 million.  Of course, prevention of pollution equates to
prevention of environmental damage.

    If we are to develop an effective means of preventing spills of oil
or  other hazardous material, we  need  first to understand the nature and
causes of such  spills.   Why do they occur?  Where?  What kinds?  How
big?  Some of this information is already at hand; for example, a review
of  both state and federal reports suggests there are four major causes
of  spills:   (1) human error, generally considered the greatest single
cause of pollution incidents;  (2)  inadequate operational procedures or
handling of hazardous materials;  (3)  poorly designed, inadequate, non-
existent, or faulty equipment; and  (4) acts of nature.  Data on other
aspects of spill causes  and nature have been reported by Battelle
Memorial Institutef^, Arthur D. Little, Inc.[2] and Dillingham.[3]

    Much data remain  to  be gathered or developed.  Once these data have
been  translated into methods and equipment, the equipment must be in-
stalled and the methods  must be  applied.  Systems must be human engineered
to  make them easy to  operate.  An on-going educational process must be

-------
instituted to make sure operators know how and why to use equipment
properly.  A system of checks must be maintained to monitor operational
procedures.  Regulations and construction codes must be drawn up and
enforced.  A device will not be useful unless it is used; an alarm will
not be effective unless it is heeded.
B.  THE SPILL PREVENTION PROBLEM


    Spill prevention is primarily a materials handling problem of storing,
transferring, or processing liquids.  Even when the potentially hazardous
substance is a solid it must often be handled in solution form or brought
into solution through contact with the water environment.

    Although the greatest number of widely publicized spills have occurred
in the transportation phase of the petroleum industry, we have addressed
problems of spills of hazardous polluting substances as well as oil at
industrial sites for several reasons:

    1.  Spills of hazardous substances have been given much less
        attention than spills of petroleum products, probably
        because of their lower visibility and volume.

    2.  The spill potentials and problems of the transportation
        industry have been approached in detail through the devel-
        opment of codes and regulations, especially from the view
        of personnel and property hazards.

    3.  Industrial facilities are less uniformly regulated than
        transportation; a greater diversity of practices and systems
        are needed for the prevention, detection and control of
        spills.

    In  industrial operations handling or processing liquids which become
hazardous polluting substances upon entry into the water environment,  a
number  of practices and systems are found for the prevention, detection
and control of spills or leaks.  Many of these were installed for rea-
sons  other than environmental pollution—e.g.

    •   Personnel protection
    •   Property protection
    •   Compliance with fire and safety codes
    •   Preventing product loss because of its dollar  value

Furthermore, each industrial facility, by virtue of  its  geographical,
topographical and climatological characteristics will have  some  unique
facets which will lead to unique spill prevention  techniques not appli-
cable at similar plants  at different locations.   The process  industries
have  developed spill prevention techniques with varying  degrees  of
                                    10

-------
sophistication, depending upon the specific materials handled, plant
locations, and process requirements.  Nevertheless, any useful appli-
cation of technology to prevent, detect, and control spills must be
based on broad principles of equipment design and operating procedures
and practices.

1.   Spill Areas

     The handling and processing of liquids are difficult to categorize
precisely for the purposes of establishing designs and developing pro-
cedures for preventing or controlling spills.  However, we believe
that four main areas of plant operations can be considered:

     •  Storage
     *  Transfer
     •  Loading and unloading
     •  Processing

These are characterized in this report as follows:

     The Storage area is, virtually without exception, where the
greatest volumetric containment of liquid occurs.  It is the area which
performs the prime function of providing for the reoccurring high
volume movement of liquids between plant and transport, as contrasted to
continuous and comparatively low volume flow of liquid to and from
processing areas.  In the storage area, spills are more frequently of
large volume due to operational inattention or catastrophic failure and,
as a consequence, are more damaging upon entry into water courses.

     The Transfer area of a liquid handling facility comprises pipe-
lines and the associated pumps, valves, and controls required in the
transfer function.  Spills are almost always the result of equipment
failures in unattended areas.  In this report, we refer to transfer
area as pipelines or conduits through which liquids flow.  Making con-
nections with and discharging into tanks and permanent or temporary
storage facilities is considered to occur in the loading and unloading
area.

     The Loading and Unloading area may be thought of as the interface
through which incoming raw materials and outgoing products pass.  This
area is often the terminus of transfer pipelines which connect to raw
material and product storage tanks.  As a consequence, large volumes of
liquids must be routed and the many temporary connections required in the
operation is a major problem.

     A Processing area consists of equipment and facilities in which
raw materials are converted into products.  In this area the major spill
problems are associated with the innumerable pumps, valves, instruments
and equipment failures associated with the physical and chemical changes
being carried out.
                                  11

-------
     Another area for spills is the waste treatment area.  However, a
waste treatment facility is often a means for preventing spills in other
locations from reaching the water resources.

2.   Spill Potentials

     The potential and magnitude of spills and leaks from the major areas
discussed above is dependent upon a number of variables and these can-
not be generalized easily.  However, there appear to be five major factors
contributing to the quantitative description of spill potential.  (See
Table 1.)  First is the inventory volume of liquid since the larger the
volume, the greater the potential hazards to a water environment  from
a spill.  A very low spill potential exists because of inventory  effects
in a loading and unloading area while a very high potential exists in
the storage area.

     The second descriptor of spill potential is the frequency of
operating cycles.  Significantly greater potential exists at the beginning
and ending of operational cycles due to a variety of reasons including
mechanical ones such as the danger of loose connections, and operational
ones such as unsteady state conditions.  A third descriptor of great
importance in loading and unloading areas is the high ratio of temporary
to permanent connections.  Each time a pipeline is connected or discon-
nected,  the potential exists for improper pipe fit, and for damage and
wear to  the pipe connectors.  In contrast, since a permanent connection
is made  only once and often hydraulically tested before use, the  low
ratio of temporary to permanent connectors gives the transfer,airea of ,a
plant a  low potential for spills.,  ,            .             	'

     The volumetric rate at which liquids are moved to and from storage
and processing  areas can cause a high spill potential to exist, e.g.,
in the unloading of supertankers where transfer rates of 10,000 to 20,000
tons per hour may occur.  Obviously, a pipeline break which is not
quickly  detected can result in spilling large volumes of liquids.  The
ubiquitous human factor in spills must be considered a very important
descriptor of spill potentials.  The greater dependence upon the  human
factor in general, the higher the spill potential.  An overall ranking
of the spill potential of the four areas suggests that loading and un-
loading  and storage areas represent the highest spill potential,  followed
by processing and transfer operations.
 C.    APPROACH


      Our investigation consisted  of  three parts—survey and analysis
 of  the  regulatory,  trade,  and  technical  literature; field  survey  and
 cvalaa.t. -t  c± trlfe  state cf the art of  spill prevention, detection and
 i-^.itt;:! ;fccrmoiogy;  auu anaL>,.u  and development of a prototype plan
 describing  fu«:v_s  .-arses  of action  for  the ^uviionmental  Protection
                                  12

-------
                                 TABLE 1

         MATRIX FOR CONTRASTING AND RANKING THE MAIN FUNCTIONS
                 OR AREAS IN LIQUID HANDLING FACILITIES
Inventory of
Contained Liquid

Frequency of
Operating Cycles
Ratio:
Temporary Con-
nections	
Permanent Con-
nections
                                                Loading &
                         Storage     Transfer   Unloading   Processing
                 Very High   Low
                       Very Low    Low
                 Low
            Moderate   Very High   Moderate
Very Low    Very Low   Very High   Moderate
Dependence Upon
Human Factor-

Volumetric
Transfer Rate

Overall Spill
Potential
                 High
                 Low
                 High
            Low
            High
Very High   High
High
            Moderate   High
Variable
            Moderate
                                    13

-------
Agency to further the "spill prevention" concept.  We focused on acci-
dental spills and leaks of oil and other hazardous materials from large
and small industrial facilities.  Only modest attention was paid to off-
shore and  onshore petroleum production because these areas are so large
and complex, and have a separate technology base, that they are beyond
the scope of our present work.

     We examined federal regulatory literature and the rules and orders
of agencies such as the Environmental Protection Agency, U. S. Coast
Guard, U. S. Geological Survey, Maritime Administration, and the Corps
of Engineers.  Letters were written to over 30 state pollution control
and health agencies requesting information on rules, regulations and orders
pertaining to prevention of spills of oil and other hazardous materials.
Fire marshalls of several states and municipalities were contacted.  We
reviewed the existing regulations to determine which provisions addressed
spill prevention—design criteria, "fail-safe" equipment, and procedures.
This survey was complemented by personal visits and telephone contact with
several state agencies.

     We briefly examined the causes of spills reported in the literature,
the corrective actions taken, and preventive measures which might
eliminate these potential hazards in other facilities.  Our attention
was focused on chronic spills of oil and hazardous materials at indus-
trial facilities because many reviews presented at oil pollution control
conferences and reports in the open literature have discussed the major
oil spills.[41  [51

     Our review of  the technical and trade literature was limited to
the last several years' publications.  We examined publications of trade
associations such as the American Petroleum Institute and Manufacturing
Chemists Association; trade and technical journals such as the Oil and
Gas Journal, Journal of Waste Water Treatment, and Chemical Engineering;
and abstract indices such as Chemical Abstracts and Index to Government
Reports.  Although  much literature was available from manufacturers, most
of it described oil detectors, valves, level indicators, alarms, etc.
We did not  feel that an extensive review of such equipment was warranted—
more important  is the general knowledge that these devices are available
on the open market.

     In our  field survey, we visited 23 large and small facilities in
the petroleum refining, oil storage and distribution, petrochemical,
organic and inorganic chemical, plastics and rubber, and metal products
industries. (See Table 14.)  The survey was conducted in four locations	
Houston, Texas; Los Angeles and San Francisco, California; the New York-
New Jersey  area; and the Illinois-Michigan area—representative of the variety
of geographical climatological, and industrial ranges encountered in the
United States.  Visits to these facilities were arranged through the
Regional Offices of the Environnental Protection Agency, State Pollution
Control Agencies, and our own personal contacts in industry.
                                  14

-------
     The objective of these visits was to obtain information about the
level of spill prevention technology actually practiced in industrial
facilities and information about how spill prevention techniques might
be improved or further developed.  Information exchange was facilitated
by our agreement with industrial representatives not to "single out" by
name specific organizations with limited or inadequate prevention pro-
grams, nor to disclose past problems with spills or present hazards, but
to focus on existing prevention techniques and how industry and government
can cooperate to improve the present situation.

     Field surveys at working facilities were supplemented by visits
to five architect-engineering firms active in the design, development
and construction of industrial facilities. (See Table 14.)  These dis-
cussions helped to identify the types of design criteria and equipment
for spill prevention that are used in new plant construction.  We also
visited with  several state and municipal water pollution control
agencies to determine their view of present pollution prevention practices,
The information gained from these visits was reviewed and summarized in
terms of the  design criteria, equipment, operational procedures, and
practices used to prevent spills in the storage, transfer, loading and
unloading, processing, and waste treatment of oil and hazardous materials.

     The last part of our program was the preparation of a prototype plan
for Environmental Protection Agency action.  Several approaches were
considered—development and promulgation of new rules and regulations,
methods for determining the hazards and spill prevention requirements
of specific industries; educational programs for industry management and
operational personnel; spill prevention demonstration programs; and
determination and development of additional equipment required for spill
prevention.   It was clear from our visits to industrial facilities that
a broad range of spill prevention technologies is being practiced
depending upon the type, size, age, and location of the facility as well
as the materials handled.  Thus, we had to c^.isider programs which are
sufficiently  flexible to be feasible within the diverse industrial
spectrum, yet lead to a more uniform and effective spill prevention
practice.

     Regulations must be enforceable, procedures must be adaptable to
specific industries, equipment must be usable in both old and new facili-
ties.  Thus,  our efforts were directed to development of a plan which is
guided and enforced by government, implemented and accepted by industry,
and provides  the necessary spill prevention  for  environmental  protection.
The prototype plan is given in Volume II of this report.
                                    15

-------
            III.  LAWS AND REGULATIONS FOR SPILL PREVENTION
     One objective of this program was to review the status of laws,
rules, and regulations pertaining to the prevention and control of spills
of oil and hazardous polluting substances.  Because of the multi-agency
jurisdiction over spills of oil and hazardous materials, we examined laws
and regulations of federal, regional, state, and municipal water quality
and health agencies.  We requested information on pertinent laws, regula-
tions and orders from 30 state water pollution regulatory agencies, 20
individual environmental engineers at state agencies, 17 state or city
fire marshalls, 6 intergovernmental groups and 23 industry associations.
(See  listing given in Appendix A.)  We also reviewed pertinent regula-
tions of the United States Geological Survey for offshore  petroleum
wells, the Hazardous Materials Regulation Board of the Department of
Transportation Bureau of Land Management, rules of regulatory agencies in
oil producing states, and fire and insurance underwriter codes.

     This review established that:   (1) most laws and regulations are
directed toward the protection of personnel and property from the
consequences of spills of oil and hazardous substances, (2) the regula-
tions for maintaining water quality consider detection, surveillance,
and cleanup of spills once these have occurred, but rarely specify
detailed prevention measures, (3) most regulations are concerned with
oil spills; other hazardous materials are mentioned infrequently.  These
conclusions are amplified in the discussion on thfe following pages.
A.   FEDERAL REGULATORY PRACTICE
1.   Federal Water Pollution Control Act

     The Federal Water Pollution Control Act clearly recognizes the
requirements for prevention within the overall concept of water quality

     "Section.  1.  (a) The purpose of this Act is to enhance the
     quality and value of our water resources and to establish
     a national policy for the prevention, control, and abate-
     ment of water pollution."

     "...it is  hereby declared to be the policy of Congress to
     recognize, preserve, and protect the primary responsi-
     bilities and rights of the States in preventing and
     controlling water pollution..."

     "Sec. 4.  (a) The Secretary shall encourage cooperative
     activities by the States for the prevention and control
     of water pollution..."
                                   17

-------
These provisions both recognize the need for prevention and indicate that
a joint federal-state effort is desirable and required for the prevention
of pollution.  The provisions listed below call for research investigation,
training and dissemination of information on the subject of prevention of
pollution:

     "...conduct in the Department of the Interior and
     encourage, cooperate with, and render assistance to
     other appropriate public (whether Federal, State,
     interstate, or local) authorities, agencies,  and
     institutions, private agencies and institutions, and
     individuals in the conduct of, and promote the
     coordination of, research, investigations, experiments,
     demonstrations, and studies relating to the causes,
     control, and prevention of water pollution."

     "...provide training in technical matters relating to
     the causes, prevention, and control of water  pollution
     to personnel of public agencies and other persons with
     suitable qualifications."

     "...collect and disseminate basic data on chemical,
     physical, and biological water quality and other infor-
     mation related to water pollution and the prevention and
     control thereof."

     "...enter into contracts with, or make grants to, public
     or private agencies and organizations and individuals for
     (A) the purpose of developing and demonstrating new or
     improved methods for the prevention, removal, and control
     of natural or man made pollution in lakes..."

Note that training is recognized as an important aspect of water pollution
control.  As demonstrated elsewhere in this report, many pollution inci-
dents are the results of human error.  Some of these could be eliminated
through training programs, either industry or government sponsored, that
point up the importance of each individual in the  total prevention program.

     The Act clearly indicates that discharges of  oil should be prevented.

     "...the Congress hereby declares that it is the policy
     of the United States that there should be no  discharge
     of oil into or upon the navigable waters of the United
     States, adjoining shorelines, or into or upon the waters
     of the contiguous zone."

The Act continues to specify penalties for persons discharging oil, to
provide for the National Contingency Plan, and contains provisions for
                                   18

-------
cleanup and control of oil pollution.  The requirements for new regula-
tions on prevention are cited in Section 11  (j), as follows:

     "...Consistent with the National Contingency Plan...,
     the President shall issue regulations consistent with
     maritime safety and with marine and navigation laws...,
     (C) establishing procedures, methods, and requirements
     for equipment to prevent discharges of  oil from vessels
     and from onshore facilities and offshore facilities..."

Section 12, which deals with control of hazardous polluting substances,
provides for the designation of hazardous substances and methods for
removal of  these materials.

     "Sec.  12.  (a) The President shall develop, promulgate,
     and revise as may be  appropriate, regulations  (1) de-
     signating  as hazardous substances, other than oil as
     defined in Section II of this  Act, such elements and
     compounds  which, when discharged in any quantity into
     or upon the navigable waters of the United States or
     adjoining  shorelines  or the waters of the contiguous
     zone,  present an imminent and  substantial danger to  the
     public health or welfare, including, but not limited
     to fish, shellfish, wildlife,  shorelines, and beaches;
     and  (2) establishing, if appropriate, recommended
     methods and means  for the removal of such substances."

     Under  Section 12 the  President is also  to study methods  and mea-
 sures  for  controlling hazardous substances to prevent discharge.  Under
 the provisions  of  the Federal Water Pollution Control Act, the designation
 of hazardous substances is proceeding.

 2.  Executive  Order  11507

     Under Executive  Order 11507,[7]  the federal  government is charged—
 in the design,  operation  and maintenance of  its facilities—with pro-
 viding leadership  in  the  nationwide effort to protect and enhance the
 quality of our  air  and  water resources.  Two parts  of this Executive
 Order  are  important  statements relating  to  the prevention of  pollution
 by oil and hazardous  materials:

      "...Heads  of  agencies shall  ensure  that all  facilities
     under their  jurisdiction are designed,  operated, and
     maintained so  as to  meet the following  requirements:
      (2) Actions  shall  be taken  to  avoid or  minimize wastes
      created  through  the  complete cycle  of operations of
     each  facility."
                                   19

-------
     "(4)  The use,  storage,  and handling of all materials,
     including but  not limited to,  solid fuels, ashes,
     petroleum products,  and other  chemical and biological
     agents,  shall  be carried out so as to avoid or minimize
     the possibilities for water and air pollution.  When
     appropriate, preventive measures shall be taken to
     entrap spillage or discharge or otherwise to prevent
     accidental pollution."

These can be interpreted as  calling for an evaluation of operations (i.e.,
processes, procedures, equipment, etc.) at each facility to avoid or mini-
mize waste and thereby minimize the waste pollution problem.  They
also imply a "fail-safe" concept, i.e., preventive measures to entrap
spillage or discharge or otherwise  prevent accidental pollution.  These
two sections, if expanded and applied to industrial facilities, would be
a major force in preventing  pollution by oil and hazardous materials.

3.   United States  Department of the Interior

     Some of the most specific regulations for preventing pollution
from accidents have been promulgated by the Department of the Interior's
U. S. Geological Survey in regulations concerning the conduct of mineral
operations and developments  in the  Outer Continental Shelf (30 CFR Part
250).[8,9]  in addition, these regulations are made a part of the leasing
program administered by the  Bureau  of Land Management as outlined in 43
CFR, Part 3380.[10]  The outer Continental Shelf Orders have been issued
by the Gulf Coast and Pacific regions of the Branch of Oil and Gas
Operations, Conservation Division of the U. S. Geological Survey.  The
intent of these orders in each region is similar; however, the specific
conditions and language employed varies.  Although these orders are
specifically addressed to oil, gas  and sulfur producing wells on the
Outer Continental Shelf, we  found these to contain more specific con-
ditions and procedures useful in preventing and controlling spills than
in any other federal regulations and have recorded in the following
Table 2 the ones we judge as most pertinent.

4.   Department of  Transportation

     The Hazardous  Material  Regulation Board of the Department of
Transportation has  established safety regulations for the design, con-
struction, operation, and maintenance of pipelines carrying hazardous
materials and petroleum products in liquid form.  These regulations are
issued as 49 CRF, Part 195—Transportation of Liquids by Pipelines.
These regulations fall into  the following categories:

     •  Sub Part A - General
     •  Sub Part B - Accident Reporting
     •  Sub Part C - Design  Requirements
     •  Sub Part D - Construction
     •  Sub Part F  - Operational Maintenance
                                   20

-------
                                                TABLE  2
                     UNITED 5TATEV. GEOLOGICAL S'JRVKt -OLTE-. CONTHSE'ITAL SHELF RECVLAUJNS.
                                                         UNITED STATES GEOLOGICAL SURVKY
Items
1. Well Casing and Cementing
   A. Drive or Structural Casing
   B. Conductor and Surface Casing
        Specific Depths
   C. Intermediate Casing
   D. Production Casing
   E. Pressure Testing
2. Blowout  Prevention
   A. Equipment
   B. Mud Program
3. Plugging and Abandonment of Wells
Gulf Coast Region

OCS No. 2—Item 1A
DCS No. 2—Item IB
OCS No. 2—Item IB
OCS No.2—Item 1C
OCS No.2—Item ID
OCS No.2—Item IE

OCS No. 2—Item 2
OCS No.2—Item 3
OCS No.3
 4. Storm Choke  or  Similar  Subsurface  Safety Device OCS No.5
 5. Procedure  for Completion  of  Oil &  Gas Wells
 6. Pollution  and Waste  Disposal
   A.  No Oil  into  Water
   B.  No Harmful Liquid Waste into Water
   C.  All  Pollution Control  Equipment Must Be
                                   Maintained
   D.  All  Platforms & Structures,  Curbed and
                     Drained  to  Tank or Sump
   E.  Operating Personnel  Thoroughly  Trained
   F.  Pollution Inspections  (Manned-Daily,
OCS No.6

OCS No.7—Item LAI
OCS No.7—Item 1A2

OCS No.7—Item 1C1

OCS No.7 —Item 1C2
OCS No. 7—Item 1C3
                             unattended-frequently) OCS No.7—Item 2A
    G.  Reporting  of Spills  and Leaks
    H.  Spill Emergency Plan—Corrective Action
    I.  Spill Control Equipment
       1.  Booms
       2.  Skinning Apparatus
       3.  Approved Dispersants
    Production Platform Requirements
    A.  Gas Detector and Alarm  System
    B.  Approved Fire Fighting  System
    C.  High and Low Level or Pressure  Alarms and
        Shutdown; Devices in all Production Vessels
          and Water Separation Devices
    D.  Remote and Local Automatic Platform and
        Well Shutdown Devices
OCS No. 7—Item 2B
OCS No.7--Item 3A1

OCS No.7—Item 3B
OCS No.7—Item 3B
OCS No.7—Item 3D

OCS No.8—Item 2A7
OCS No.8—Item 2A6

OCS NO.8—Item 2AI

OCS No.8—Item 2A2
    E.  High 4 Low Pressure Oil  Pipeline Alarms
        &  Control Devices  to Shutdown Shipping Pumps
        &  to Shut in all Well in Event of Actuation OCS No.9—Item LAI
    F.  Approved  Sewage  Disposal System
    G.  Auxiliary Power  Supply Equipment
    H.  Approved  Waste Water  Handling  and
        Disposal System
 8.  Gathering  Pipelines
    A.  Automatically  Controlled Shutoff Valves
    B.  Corrosion Protection
    C.  Check Valves
    D.  Other Spill Preventing Equipment
OCS No. 8— Item 2A9
OCS No.8--Item 2A4

OCS No. 8 — Item 2AS

OCS No. 8— Item 2A2
 Pacific  Region

 OCS No.10—Item 1A1
 OCS No. 10—Item 1A2
 OCS No. 10—Item lA2-ii
 OCS No.10— Itrm 1A4
 OCS No.10—Item 1A5
 OCS No. 10—Item 1A6

 OCS No. 10—Item 1B1
 OCS No.10—Item 1C
 OCS No.3
 OCS No.10—Item 2
 OCS No.6

 OCS No.7
 OCS No.7
 OCS No. 10—Item 5-7
OCS No. 8— I td
               2A2
OCS No.10—Item 6
OCS No. 10—Item 6
OCS No. 10—Item 6

OCS No. 10—Item 5-1
OCS No. 10—Item 5-2

OCS No. 10—Item 5-3

OCS No. 10—Item 5-4

OCS No. 10—Item 5-5
OCS No. 10—Item 5-6
OCS No. 10—Item 5-8

OCS No.10 —Item 5-9

OCS No.10—Item 3-1
OCS No. 10—Item 3-2
OCS No.10—Item 3-3
OCS No. 10—Item 3-4
                                                    21

-------
While these regulations include many standards which are principally
responsible for insuring that adequate safety precautions are realized
in design, construction, operation and maintenance of pipelines,  the
only portion directly pertinent to pollution control is the requirement
of telephonic notice of leaks at the earliest practicable moment  following
discover)'' that resulted in pollution of any stream, lake, river,  or other
similar body of water.
B.   STATE AND REGIONAL REGULATORY LITERATURE
     Within the scope of the present study it was not possible  to
investigate the latest regulatory literature of all states in great detail.
As a preliminary exercise, we reviewed the State Water Quality  Laws, as
compiled in the Environment Reporter issued by the Bureau of National
Affairs, Inc., to determine which state agencies have specific  authority
to regulate spill prevention techniques.  The types of regulations and
the fraction of states which have regulations are shown below:

                                                            % of States
                                                            with these
                 Types of State Regulations                 Regulations
      1.  Develop programs for treatment and disposal            48

      2.  Establish Water Quality Standards                      60

      3.  Examine plans and give approvals for wastewater        64
         treatment

      4.  Issue permits, determine compliance, and revoke        92
         permits

      5.  Adopt rules  and regulations to abate and prevent       68
         pollution

The pertinent information for each  state is given in Table 3.  Although
over  2/3 of  the states have  regulations which cover pollution abatement
only  a few have specific regulations pertaining to spills of oil and
hazardous  materials.  Table  4 indicates those states for which specific
spill regulations were found as the result of direct inquiries  (see
Appendix A for list of contacts and responses) or from information
received during field interviews.   From this review, we conclude that
pollution  by discharge of oil or petroleum products is addressed in
greater depth and more frequently than pollution by hazardous materials
While major  oil producing states have specific regulations concerning
production of oil and the prevention of oil pollution during product
a limited  number of states have recognized the potential for pollut'   '
                                    22

-------
TVPKS OF STATK WAT1.K I'OLUTIOH K1CULATIONS
Alabaioa
Alaska
Arizona
Arkansas
California
Colorado
Connecticut
Delaware
Florida
Georgia
Hawaii
Idaho
Illinois
Indiana
Iowa
Kansas
Kentucky
Louisiana
Maine
Maryland
Massachusetts
Michigan
Minnesota
Mississippi
Missouri
Montana
Nebraska
Nevada
New Hampshire
New Jersey
New York.
New Mexico
North Carolina
North Dakota
Ohio
Oklahoma
Oregon
Pennsylvania
Rhode Island
South Carolina
South Dakota
Tennessee
Texas
Utah
Vermont
Virginia
Washington
West Virginia
Wisconsin
Wyoming
Develop
Programs tor
Treatment
'and Disposal
X


X
X
X
X
X
X
X






X



X


X

X
X

X



X
X
X
X
X

X


X
X

X



X

Eat.-.bllsli
Water
Quality
Standards
X
X

X
X

X

X
X

X

X
X
X
X
X



X
X


X



X

X
X


X
X

X
X
X
X
X
X

X


X
X
Examine Haass
and Approve
WjstevatPT
Treatment Pitas
X

X



X




X


X

X

X

X

X

X

X

X
X
X
X
X
X
X
X
X
X
X

X
X
X
X
X
X
X
X
X
X
Issue Permits
Determine
Compl innce,
Revoke Permits
X
X
X
X

X
X
X
X
X
X

X
X
X
X
X
X
X

X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X

Ailopt Rules 4
Regulations
to Abate & Pre-
vent Pollution

X
X
X
X
X

X
X
X
X
X

X


X
X

X

X

X
X
X
X
X
X
X
X
X
X
X

X
X
X
X
X




X
X



X
              23

-------
                                 TABLE 4

                    SPECIFIC STATE SPILL PREVENTION,
                      RULES, REGULATIONS AND LAWS
                      Spill Prevention Regulations

                                                        National or Local
State                 OH           Other than Oil      Contingency Plan

Alaska                 X                  X
California                                                      X
Colorado         Reporting only
Florida          (in Litigation)
Louisiana              X
Maine                  X
Maryland         In Preparation
Massachusetts    Filed
Michigan                            Being Considered            X
Nebraska               XX                     X
New Jersey                                X             Being Adopted
New York               X                  X
Pennsylvania                              X
Rhode Island           X
Texas                  X
Wisconsin              X                                Planned
                                    24

-------
by oil and hazardous materials during  transport and at terminal operations
by providing both guidelines and in some cases specific procedures to pre-
vent pollution.  The most l pertinent and applicable state regulations for
spill prevention, including those which provide for specific procedures,
methods and equipment  for preventing spills of oil and hazardous materials,
are reviewed on  the following pages.

1.   Specific Preventive Measures

     The  regulations of several state  agencies describe specific pro-
cedures,  methods, and  equipment to be  used for preventing spills of oil
and hazardous materials.  Some of these are reviewed below.

     The  Rhode  Island  Department of Healthful provides many specific
regulations  concerning procedures and  equipment pertaining primarily to
transfer  of  oil from a vessel  to shore or from shore to vessel, and at
storage and  terminal operations.  Some examples of the regulations are
the pressure testing of  flexible hoses used in transfer operations, the
use of drip  pans under hose  connections, proper support for hoses and
sufficient length to avoid any strain, illumination of wharves or pier
areas  during transfer  operations, check valves in discharge lines, closing
of valves in dike surrounding  tanks, storage  tank inlets, overflows and
vents, etc.   Because of  the  broad scope of these regulations, they have
been  reproduced in Appendix  B.

      Massachusetts' Division of Water  Pollution Control I 12 J has filed
rules  pertaining to marine oil transfer operations, terminal and bulk
plants and other oil handling  installations,  spills, and other accidental
discharges.   The marine  oil  transfer operation specifies procedures and
equipment such as:  plugging of scuppers, blanking ends of hoses, drip
pans,  checking connections,  flanges and joints, curbs on, wharves or piers,
etc.   Other parts of  the  regulations require  dikes or retaining walls
around  tanks or tank batteries, use of oil traps in terminal areas,
and  granting of licenses  to  terminal operations.  Parts of these regula-
tions are included in  Appendix C,
      Alaska, 13  j_n its oil and gas conservation regulations  and  statutes,
 provides for prevention of leaks and breaks  in wells  and  piping as well
 as other prevention measures.   There is also a list of  regulations per-
 taining to the prevention of industrial waste pollution.   General guide-
 lines are given for industries as varied as  meat packing  plants and
 canneries, metal industries, and pulp and paper mills.  Most  of these
 regulations ; ":a general but specific procedures for oil separation and
 collection are given.   The broad potential of these regulations is illus-
 trated by the section entitled "Oil Transportation Equipment."

      "...Tankers, railroad tank cars, tank trucks, or other
      facilities and for the loading, unloading, storage,  and
      transportation of oil shall be equipped for the  collec-
      tion of the drips from hose cr ether connections and
                                   25

-------
     the excess oil contained in hose and pipelines, wherever
     there is a possibility that this oil will find its way,
     either directly or indirectly,  into a body of water.
     Provision shall be made, also,  for catching accidental
     spills, and these facilities shall be of such a capacity
     as to hold the maximum quantity of oil  possible from
     any one spill."

The provision indicates that facilities should be available to hold the
maximum quantity of oil that could be released in any spill; implementa-
tion of such regulation could prevent many accidental spills which might
otherwise make their way to the water.

     Louisiana's Stream Control Commission has rules governing disposal
of waste oil, oil field brine, and all other materials resulting from the
drilling for, production of, or transportation of oil, gas or sulphur. U^J
The most pertinent of these from the viewpoint of spill prevention are as
follows:

     "1.  Crude oil, waste oil, oil sludge, oil-water emulsion,
     or oil bearing mixtures of any kind shall be gathered and
     destroyed by burning or otherwise on the lease where the
     wastes originate, and in such manner as to eliminate any
     pollution hazard.

     "2.  No oily fluids shall be discharged to, or allowed
     to flow on the ground, or be carried from the original
     lease in open ditches, or discharged or allowed to flow
     into any stream, lake or other body of water."

     "3.  a. Each producing well, except those over marsh
     and water, all oil booster pumps, and any pump used to
     move oil or oily fluids, shall be provided with a sur-
     rounding gathering ditch or equally effective device,
     to prevent the escape of oily wastes from the location,
     such ditch to be graded to a gathering sump which shall
     be cleaned regularly by removal and destruction of oily
     wastes.  All spillage of oil shall be promptly gathered
     and destroyed.

          b.  On all pumping wells,  over water or marsh,
     there shall be installed an adequate impervious deck
     or other device with a catch tank installed around the
     wellhead.  The catch tank should be equipped with a
     "stiff-leg" to enable the operator to dispose of
     excess rainfall.
                                  26

-------
     c.  All drilling barges, whether for workover or
drilling new wells shall be equipped with a device
at the open end or ends of keyways to prevent oil or
oil fluids from escaping therefrom.  This device
shall be so installed as to be adjustable for tidal
changes and all oil collected within keyways shall
be picked up and disposed of in compliance with para-
graphs 1 and 2."

"4.  Each permanent oil tank or battery of tanks that
are located within the corporate limits of any city,
town, or village or where such tanks are closer than
500 feet to any highway or inhabited dwelling or
closer than 1000 feet to any school or church, or
where such tanks are so located as to be deemed a
hazard by the Stream Control Commission, must be
surrounded by a dike (or fire wall) or retaining
wall of at least the capacity of such areas where
such dikes (fire walls) or retaining walls would be
impossible such as in water areas.  At the discretion
of the Stream Control Commission, fire wall of 100%
capacity can be required where other conditions or
circumstances warrant their construction. (As
Amended December 13, 1964.)  Tanks not falling in
the above categories must be surrounded by a retain-
ing wall, or must be suitably ditched to a collecting
sump,  each of sufficient capacity to contain the
spillage and prevent pollution of the surrounding
areas."

"5.  Oil gathering lines, or any other lines used for
transporting oil, shall be regularly inspected and all
leaks  shall be immediately repaired.  Waste from leaks
shall be collected and destroyed immediately upon dis-
covery.  All barges used for the transportation of
crude oil or petroleum products shall be in first class
condition.  Leaking barges shall be repaired before reuse.
Loading racks, barge-loading outlets, and similar instal-
lations shall be operated at all times with full precau-
tion against spillage.  Such installations shall be sur-
rounded by a ditch graded to a gathering sump, or shall.
be provided with an impervious deck surrounded by a steel
gutter leading to a sump, or with such other equipment
adequate for the accomplishment of the same purpose as
may be approved by the Stream Control Commission.  All
such gathering sumps shall be cleared regularly by re-
moval and destruction or other safe disposal of the oily
waste.  After each operation of barge or tanker loading
equipment, loading hose and connections shall be care-
fully drained, and the gathering sumps shall be emptied,
preferably to the barge or tanker."
                               27

-------
     In Texas, Statutory Authorization, Article 7621d, Section 10(c)(4),
places sole responsibility on the Railroad Commission of Texas for  the  con-
trol or disposition of waste, and abatement and procedures of pollution of
water, both surface and sub-surface, resulting from activities associated
with the exploration, development, or production of oil or gas.  The com-
mission issues its rules and regulations under the title "General Conserva-
tion Rules and Regulations of Statewide Application, State of Texas".lljJ
Many of these are similar to those of the USGS's Outer Continental  Shelf
Regulations.  The directly applicable regulations are found in Rule 8,
Water Protection given in Appendix D.

     The following four state laws specifically apply to prevention of
discharge of hazardous materials and other wastes and provide a mechanism
for state regulation of prevention and control procedures.

     State of New York.  Item 13, Section 10, Article 2 of
     Chapter  140 of the Laws of New York.  "The Department
     of Environmental Conservation...shall have power to:
     13, Prevent pollution through the regulation of the
     storage, handling, and  transport of solids, liquids and
     gases which may cause or contribute to pollution."

     Commonwealth of Pennsylvania.   Section 402, Potential
     Pollution, Article IV,  Clean Stream Law as Amended,
     July  31, 1970.

           a.  Whenever the board  (Department of Environmental
     Resources) finds that any activity, not otherwise requir-
      ing a permit under this Act, including but not limited
      to the  impounding, handling, storage, transportation,
     processing and disposing of materials or substances,
      creates  a danger of pollution of the waters of the
      Commonwealth or that regulation of the activity is
      necessary to avoid such pollution, the Board may, by
      rule  or  regulation require that such activity shall be
      conducted only pursuant to a permit issued by the
     Department or may otherwise establish the conditions
      under which  such activity shall be conducted, or the
      Board may issue an order to a person or municipality
      regarding the particular activity.  Rules and regula-
      tions adopted by the Board pursuant to this section
      shall give  the persons  or municipalities affected a
      reasonable period of time to apply for and obtain any
     permits  required by such regulations.

      Commonwealth of Virginia.  Article 3—Regulation of
      Industrial  Establishment, Section 62.1-44.16
                                  28

-------
    1.  Any owner who  erects,  constructs,  opens,  reopens,
    expands or  employs new  processes  in  or operates  any
    establishment from which  there  is a  potential or actual
    discharge of industrial wastes  or other wastes to state
    waters shall first provide facilities  approved by the
    Board  for the treatment or control of  such  industrial
    wastes or other wastes.

    62.1-44.17"...shall upon  request  of  the Board install
    facilities  approved by  the Board  or  adopt such measures
    approved by the Board as  are necessary to prevent the
    escape,  flow or discharge into  any State waters  when the
    escape flow or  discharge  of such  other wastes into any
    State  waters would cause  pollution of  such  State waters."

    The State of Rhode Island in its  pollution  regulations
    provides  a  mechanism for  adoption of pollution prevention
    procedures, following an  incident in which  pollution has
    occurred.   This order reads as  follows:

     "••-Order to adopt pollution prevention systems  —If any
     person is  polluting the waters  of the  state,  and if after
     such investigation the director shall  so  find, he shall
    make his findings in writing to that effect and  may enter
     an order directing such person  to adopt or  use or to
     operate properly, as the  case may be,  some  practicable and
     reasonably  available system or  means to prevent  such
     pollution,  having due regard for  the rights and  interests
     of all persons  concerned.  Such order  may specify the parti-
     cular system or means to  be adopted, used or operated; pro-
     vided, however, that where there  is  more  than one such
     practicable and reasonably available system or means, such
     order shall give to the person  complained of the right to
     adopt or use such one of  said systems  or  means as he may  chose."

     Other laws  are less specific in that they prohibit pollution  but  do
not provide for  spill prevention control, for  example:

     State of Nebraska.  71-3007. Unlawful Acts

     1.   It shall be unlawful  for any person:

         a.  To  cause pollution of any waters  of the  state
     or to place or  cause to be placed any  wastes in  a
     location where they are likely  to cause pollution of
     any water of the state...
                                    29

-------
     State of New Jersey.

     4.   The discharge of  hazardous substances, debris, and
     petroleum products into or in a manner which allows flow
     or  runoff into or upon the waters of this State and the
     banks or shores of said waters is prohibited.

     From this review of state water quality laws we conclude that
specific legislation permitting regulatory bodies to establish rules and
regulations directed at methods for preventing spills from occurring and
from entering water courses is inadequate to insure that the handlers of
hazardous polluting substances are taking actions necessary to prevent
spills of hazardous substances from polluting the Nation's water resources.
C.   FIRE LAWS AND FIRE PREVENTION AND UNDERWRITER CODES
     The laws and regulations for fire protection are primarily for
protection of people and property,  especially in the handling of flammable
liquids.  Although the requirement  of dikes  around any tank storing
flammable liquids is an excellent regulation from the viewpoint of
preventing widespread pollution upon rupture of  a tank,  the reasons for
this requirement are solely for protection of people and property.  Conse-
quently, fire laws and codes can be considered as valuable but specific
adjucts to rules and regulations required to decrease the potential for
spills of hazardous substances entering water courses; however, they are
only that—valuable adjuncts.
                                  30

-------
                  IV.  TECHNICAL AND TRADE LITERATURE
     We surveyed recent technical and trade literature to determine
(1) the recorded causes of spills of hazardous polluting substances,
(2) equipment, design criteria and procedures for spill prevention and
(3) indication of the extent to which techniques and equipment are used
to prevent and control spills of hazardous materials.  The results of
this survey formed a basis for establishing the direction of the plant
surveys in which we sought additional information for evaluating the
practices of industry in preventing and controlling spills.  Literature
sources for this survey are listed in Table 5 and were limited primarily to
publications of the last three years since previous work bad indicated
that prior to 1967, few articles had reported on spills of oil and hazardous
materials.  We specifically contacted 23 professional and trade associa-
tions to obtain their publications.  (See Appendix A.)
A.   CAUSES OF SPILLS
     We concentrated on obtaining information on hazardous materials
other  than oil because the  latter have been well documented and we were
' -i*? ing information on much broader types of materials.  Table 6 illus-
ti  ct?3 the types  and causes of spills.  The preventative actions that
have' been recommended by  the  investigating groups to eliminate subsequent
failures are  also listed  in Table 6.  These actions deal primarily with the
correction of equipment failures; however, consideration of the nature of
the failures  suggests that  more attention to inspection, maintenance and
general good  housekeeping could have prevented many of these accidental
spills.

     The failures recorded  in Table 6 that resulted in accidental spills
of  chemicals  are  similar  to those reported as causes of oil spills entering
the River Thames  outside  of London.[19] of 394 reported oil spills, 30%
resulted from storage of  oil, 10% from oil pipelining, 10% from the dis-
posal  of waste oil, 11% from  engines, auto service stations vehicle depots,
railroad and  air  fields,  5% from road tank-truck accidents, 23% from
general spillage, and the remaining 11% being unknown.  Of 90 small and large
spills originated from oil  storage  installations, 35 were caused by over-
filling of tanks  and 51 by  leaky valves or from valves that had been
damaged deliberately.  At least 74  of these incidents could have been
avoided if elementary precautions had been taken in designing the tank
storage area. Nearly all of  the spills from oil tanks were attributable
to  human error.   Pipeline failures were due to corrosion, a lack of catho-
dic protection, or by structural damage during road construction.  Most of
the spills in industrial  facilities were caused by careless use of oil,
spillage or improper disposal by employees.
                                   31

-------
                                TABLE 5

                    SOURCES USED IN LITERATURE SURVEY
Abstracting and Indexing Services

   Engineering Index
   Oceanic Index
   Applied Science and Technology Index
   U. S. Government Research and Development  Reports  Index
   Technical Abstract Bulletin Index
   Chemical Abstracts
   Nuclear Science Abstracts
   Air University Library Index to Military Periodicals
   Department of Interior, Office of Water Resources  Research,  Water
      Resources Research Catalog


Federal Agencies

   Government Printing Office Monthly Catalog:   GPO Price Lists,  #42,
      Irrigation, Drainage and Water Power, and  #58, Mines, Explosives,
      Fuel, Gasoline, Gas, Petroleum, Minerals
   Various Agencies and Departments:  Department of the Interior  (FWQA, USGS) ;
      Office of Water Resources Research;  Department  of Transportation (USCG) ;
      Department of Commerce (NOAA); AEC;  Council on  Environmental Quality,
      Environmental Protection Agency; National Science Foundation; Water
      Resources Council; National Council  on  Marine Resources and Engineering
      Development


Scientific and Technical Societies

   American Petroleum Institute
   American Chemical Society
   American Institute of Chemical Engineers
   American Institute of Mining, Metallurgical  and Petroleum Engineers
   American Nuclear Society
   American Society for Metals
   American Society of Civil Engineers
   American Society for Testing and Materials
   American Society of Mechanical Engineers
   Compressed Gas Association
   Manufacturing Chemists Association
   National Academy of Sciences, National  Academy of  Engineering, National
      Research Council
   American Insurance Association, Engineering  and Safety Department


Selected Journals

   Chemical Engineering                Environment
   Chemical Engineering Practice       journal  of Water Pollution Control Federation
   Oil and Gas Journal                 Pollution Engineering
   Chemical Engineering Progress       Environmental  Science and  Technology
   Ocean Oil                           Water  and Waste Engineering
   Oil,  Gas and Petrochem Equipment    Industrial Water Engineering
   Chemical and Engineering News

                                      32

-------
                                                TABLE 6

                            TYPES, CAl'SLS ASP READIES FOP CHEMICAL ?PILLS
CHEMICALS INVOLVED

Caustic Soda
FAILURE

Flexible pipe breaks loose while
loading caustic soda into tankcar
PREVENTIVE MEASURES

    Redesign loading device and install safety i/ljrcp

    Review facilities for handling hazardous ch^nic.ils
Aimonla
                             Scale tanks overfilled with
                             ammonia; relief valve popped spray-
                             ing liquid ammonia into atmosphere
                                         Install high-level alarms on scales

                                         Install high-level cut-off valve on distribution
                                         tank
Aniline
                             Aniline  stripper ruptures due to
                             plugged  vent line
                                         Install  double valves and tell-tale bleeds

                                         Install  instrumentation-!.e.  level
                                         and pressure recorders,  alarms
                                         Redesign safety seal	
Monomer
                             Tank overflow during filling; loss
                             of  13,127  Ib. of monomer; cause:
                             plugged vent pipe
                                     Inspect and  clean vent  pipe  regularly
Sulfuric Acid
                              Hose bursts during transfer of
                              acid
                                     Do not use hoses foi  sulfuric acid loading; use
                                     pipes and swivel joints
Oleum
                              Rupture  in flexible Teflon vtw hose;
                               isket failure
                                         Install expansion valve
                                         Install pressure  relief valve
 Ammonia
                              Relief valve discharged improperly
                              handled
                                         Pipe discharge to ditch

                                         Line to vent pressure to keep pressure below
                                         relief valve setting
 Caustic Potash
                              Drum overflowed into sewer;  re-
                              acted with sulfides in sewer-* H$
                                     Redesign sewers to prevent "mixing"  of hazardous
                                     materials that may react undesirably
 Caustic Soda
                              Failure of gate valve and  check
                              valve
                                         Redesign valves
                                         Redesign to prevent chemical contamination of
                                         steam and water supplies
 Aranonia
                              Leaks in two manual block valves
                              and automatic control valve
                                         Replace/repair valves

                                         More frequent inspection
 Phosphorous Acid
 Failure  of  butterfly-type valve
 due  to corrosion
    Careful inspection of system
    Possible-redesign of piping
 Phthalic Anhydride
 Tank overflow  during  filling
                                                                   Install more  reliable  level  indicators  on tanks
 Phosphorous Acid
 Sulfuric Acid
 Valve  failure  (defective valve)
Repair/replace valva
 Hose  rupture allows H2S04 to enter
 sewer
Replace with permanent piping  to appropriate  drainage
location
 Sodium Sulfhydrate
 Pump  failure;  sodium sulfhydrate
 enters  sewer
    Repair pump

    Install sump pump
 Formaldehyde
 Spring valve  failed
Replace spring valve with gate valve
 Phenol
Overloading of still due to failure
of gauge
Redesign gauges  to prevent  inaccurate  readings  due;  to
clogging
 Sulfuric Acid
 Leaking valve due  to pressure
 buildup
 Installation  of vent  line  to  relieve  pressure
 buildups
 Nitric Acid
 Sulfates
 Toluene
 Faulty  hose  connect  and leaking
 cock  In line
     Replace  hose with permanent  pipe
     Replace/repair  cock
 Hot sultatc' slurry cvtrHovs due
 to pump failure
                                                                   Investigate different pumps to handle slurry
 Sight glass in stripper  kettle  line
 failed
     Install now pressure-type sight glass

     Clean and  inspect periodically

     Redesign to eliminate  sight glass
                                                            33

-------
                                               TABLF  6  (Continued)
CHEMICALS :NVUVF.:>
Caustic Soda
Acrylonitrili
Anhydrous Ammonia
Sulfuric Acid
Hazardous, flammable
chemical in polymerization
reaction (pilot plant)
Anhydrous Ammonia
Acid Cement
Corrosive Chemical
Vinyl Chloride
Chloroacetic Acid
Acetanilide
Ammonium Nitrate
Phenol
Ammonia
Liquid Organics
Sodium Cyanide
Methyl Alcohol
Caustic and Peroxide
Unspecified Poison
Textile Waste
Industrial Waste
Adhesives
FAILURE
Failure o£ cock valve while caustic
soda being loaded
Water seals on reactor agitator
bleu
Hose ruptured a fitting
Cast iron pipe ruptures
Safety disc rupture; escaping
materials did not vent out proper
vents
Rupture of flexible hose on tank
truck
Frozen valve failed to bleed off
pressure when opened; accumulation
of cement prevented second valve
from being closed
Gate valve failure (valve stem)
Sight glass failure
Mechanical failure of valve
Valve blows under pressure
Valve failure due to pressure
buildup
Frozen valve; plugged cock
Safety valve failure; failure of
pressure gauge
Overflow of surge tank
Dumping of cleaning agent in sewer
Tank truck wreck; contents spilled
into river
Pipeline failure
Employee washed containers used
for poison storage in river
Insufficient waste treatment plant
Lagoon banks rupture
Spills into floor drains enter
river
PREVENTIVE MEASURES
Inspect cock valves before each use
Redesign cock valve
Redesign water seals
Resize reactor vents to relieve pressure without
blowing
Replace leaking block valve
Install permanent piping
Redesign piping system replacing cast iron pipes
with PTFE-llned carbon steel piping
Temperature controller Installed
Review procedures to guard against future
pressure buildups
Install check valve on tank line
Replace valves
Valves to be kept warm with use of propane heaters
Replace valves with more suitable type valves
Replace sight glass with one rated for pressures
developed in reactor
Redesign valve
New valve design
Orifice restriction to be Installed to limit flow
Inspection and repair of valves and cocks
Replace faulty valve; review design of gauge and
possibly replace with better one
Installation of alarm to signal overfill
New treatment plant constructed
~
Repair and inspect pipeline
Change housekeeping procedures
Reuse of plant waste and redesign of treatment system
Reconstruct lagoon; fence in area
Divert waste to sewage disposal system
Acid Waste
                             Breakdoum in lime  pumps  for
                             neutralization  resulted  in acid
                             v.iste discharge
Replace pump and add standby unit
    Data Sources:  References 10, 17, 18; Reports of  Accidents maintained at the South
                   Ontrai Region Office of the Environmental Protection Agency.

                                                         34

-------
     The same type of accidents and  causes  are  found  in  the  list  of
types and causes of oil spills  (Table  7)  in Rhode  Island  during the period
of July 1, 1968 to June 30,  1969,  and  for incidents taken from the Environ-
mental Protection Agency's South Central  Region Office.   Thus, we conclude
that the causes of spills are essentially the same regardless of  country
and geographical location and are  primarily related to human error, either
in design or operation.

     The best documentation  of  failures of  equipment  and  operational
errors in handling hazardous materials was  found in a systematic[20]
survey of several hundred fires and  explosions  in  the chemical industries
over the past 20 years.  On  the basis  of  these  case histories, the investi-
gators suggested a series of hazards factors as the principal causes or
contributors to these accidents.   Although  the  study  was  concerned with
fire and explosion losses, the  same  hazard  factors often  result in spills
of hazardous materials.  Those  factors that we  believe are most significant
in spills of oil and hazardous materials  are underlined  in Table  8.
Previous work[l»2>3>^J suggests that the  last four causes given in Table
8—material movement problems,  operational  failures,  equipment, and in-
effective loss prevention programs—are probably the  most important cause
of spills of oil and hazardous materials.  These hazard  factors are well
known  to  fire and safety engineers;  careful consideration of them by
environmental specialists may be an  approach to help  prevent spills.
 B.   EQUIPMENT,  DESIGN CRITERIA AND PROCEDURES FOR SPILL PREVENTION
      The results of our literature survey confirmed our  original  hypothesis
 that little specific technical information is available  on equipment  and
 design criteria solely for prevention of oil and hazardous material spills.
 Because liquid handling methods and systems are devised  from equipment
 components, the most detailed design criteria and equipment specifications
 are based on achieving certain standards of design and fabrication to
 meet specified operational conditions.   Furthermore,  the specificity  of
 these standards becomes more rigorous and the degree of  permitted varia-
 bility becomes less broad for either unusual operating conditions, e.g.,
 temperatures and pressures significantly above or below  ambient,  or where
 hazards to property and personnel are high such as from  fire or toxicity.

      Literature references on equipment are principally  restricted to con-
 tainment -and removal devices for spilled oil and not on  equipment for
 spill prevention.  We determined that the best approach  to the equipment
 aspect of spill prevention is adherence to manufacturing, construction and
 performance standards commensurate with the potential for spills to  occur
 and to enter water resources because the Iiteraturell6,17,18] indicated
 that spills could not be overcome solely through reliance on improved equip-
 ment and because of the impracticality of devising generally meaningful
 equipment configuration and designs for all spill prevention problems.
                                    35

-------
                                                         TABLE  7

                                         TYPES,  CAUSES  AND REMEDIES FOR OIL SPILLS
SPILL TYPE

Black oil in river


Black oil in river


Black oil in river


Oil at wharf

Light fuel oil at terminal

Light fuel oil


Heavy fuel oil

Heavy fuel oil


Heavy fuel oil

Light fuel oil


Bunker C

Crude oil

Crude oil

Crude oil

 SPILL TYPE

 Crude oil

 Crude oil


 Crude oil
FAILURE OR CAUSE

Vandals emptied fuel tank iAto  plant  floor  drain;
entered river

Breakdown of heating unit causes oil  to be  dis-
charged through floor drain

Break of fuel oil coupling in plant,  oil dis-
charged through drain

Improperly maintained oil spearator leaked

Leaky hatch covef

Pipeline rupture of unknown cause


Barge went aground

Overflow of storage tank during transfer; flowed
through yard drain

Improper ballasting procedure caused  spill  of  oil

Overflow storage tank, valve in diked area  left
open

Tank overflow during storage

Pipeline break caused by pile driving in area

Heater-trcater malfunction

Oil In dike from overfilled tank; dike valve open

 FAILURE OR CAUSE

 Storage tank rupture, dike valve open

 Drop in high tide resulted in  siphoning oil from
 separator

 Farmer broke pipeline while plowing  field
CORRECTIVi:  ACTION *

Place vali-e in floor drain


Use separator  for floor drain


Terminate floor  drains in dry  sump


Repair or replace separator

Mechanical  repairs

Build retaining  walls  around pipeline
and transfer pumps



Seal yard drain
Close valve; update  inspection
procedures
 CORRECTIVE ACTION *
 *  Recommended in state report.
                                                        36

-------
     PROBLEM

 1.  Plant  Siting
 2.   Plant  Layout
3.
Non-Conforming
Structures
 4.   Material Evaluation
 5.   Process
                     TABLE 3

        HAZARD FACTORS IN CHEMICAL PLASTS



                 FACTORS
•  Unusual exposure to natural forces
   such as windstorms^ floods, earth-
   quakes
•  Poor locution with respect to water
   and utility supplies
•  Hazards from nearby plants

•  Unreliable public fire and emergency
   protection
•  Difficult traffic conditions for
   emergency equipment
•  Inadequate waste and disposal facili-
   ties
•  Climatic conditions requiring indoor
   installation of hazardous processes.
•  Congested process and storage areas

•  Inadequate Isolation of extra hazar-
   dous operations
•  Exposure of high-value, difficult to
   replace equipment
•  Lack of proper emergency exits
•  Insufficient space for maintenance or
   emergency operations
•  Ignition source too close to hazards
•  Critical plant areas exposed to hazards
•  Inadequate designation of plant hazard
   areas
•  Disregard of building codes
•  Inadequate fire restrictive structural
   supports
•  Failure to provide blast walls or cub-
   icles for extra hazardous operations
•  Inadequate explosion venting
•  Inadequate building ventilation
•  Insufficient exits
•  Electrical equipment not in confor-
   maoce to required codes
•  Insufficient evaluation of fire,
   health and stability characteristics
   of materials

•  Lack of established control for
   quantities used

«  Inadequate assessment of processing
   conditions on hazardous character-
   istics
•  Lack of information on dust explosion
   potentials
*  Toxicologies! hazards not properly
   evaluated
•  Incomplete inventory of hazardous
   materials
•  Iffipror'f-r packaging and labeling
*  Lack of information on effects of
   process temperature and pressure
   vari al i^pj?
•  Lack of inf ormat i-in on hazardous by-
   products or sl;ie	react ions
•  JkiaJi^niiato knowledge of process
   r_e:.>c t^ion r^t >.>;-;_
•  Failure to Identify possible
   explosive reactions
e  Jnailfvjual:<• J?V;ili">«.J_on__of environment
•  Fail'tre to prrvKV {or extreme	process
   c.-iiidlt ions
                                                                    EXAMPLES OF 11-V,' FACTORS COULD
                                                                    	AFFECT SPILLS	
                                                                    «  Weathered contaminants could
                                                                       be washed into drains

                                                                    •  Insufficient wash water
                                                                       available
                                                                    •  Hazards could cause spill
                                                                       situations
                                                                        •  Incomplete cleanup of process
                                                                           waste
                                                                    »  Insufficient room for curbing
                                                                       or dikes
                                                                        •  Poor maintenance could lead
                                                                           to  chronic leaks

                                                                        •  Fire or explosive hazards
                                                                           could cause spills in adjacent
                                                                           areas
                                                                           Inadequate materials usage
                                                                           could yield spills, e.g.
                                                                           incorrect materials of
                                                                           construction for storage
                                                                           Excess quantities of mater-
                                                                           ials could exceed prevention
                                                                           measures, e.g. dikes, sumps
                                                                           Processing could change com-
                                                                           monly spilled non-hazardous
                                                                           materials to hazardous
                                                                       Can lead to Inadequate spill
                                                                       prevention plan

                                                                       Could lead to spills from
                                                                       process equipment

                                                                       Materials of unknown hazard
                                                                       could be spilled
                                                 37

-------
                                         TABLE 8 (Continued)
7.   Operations
6.  Material Transport   «   Lack  of  control during processing

                         •   Inadequate  controls for dust hazards
                         •   Piping problems

                         •   Improper identification of hazardous
                            materials
                         •   Loading  and unloading operations

                         •   Flammability
                         •   Heat  transfer control
                         •   Pneumatic conveyor explosions
                         •   Waste disposal and air pollution
                            problems
                         •   Lack  of  detailed operating instruc-
                            tions and procedures
                         •   Inadequate  operator training programs
                         •   Poor  supervision
                         *   Inadequate  start-up and shut-down
                            procedures
                         *   Poor  inspection and housekeeping
                            programs
                         •   Inadequate  operating permit program
                            for hazardous materials
                         •   Lack  of  emergency ccr.trol plans
                         •   Inadequate  drills in operating emer-
                            gency procedures
                         •   Hazards  inherent in design
                        •  Corrosion or erosion
                        •  Metal fatigue
                        *  Defective fabrication
                        *  Inadequate control
                        •  Process conditions exceeded design
                           limits^
                        •  Poor maintenance
                        •  Inadequate repair and replacement
                        *  Lack of "fail-safe" instrumentation
                        •  Inadequate inspection for adherence
                           to construction criteria or material
                           specifications
                        *  Lack of assigned responsibility
8.  Equipment  Failure
9.  Loss Prevention
    Program
                        *  Ineffective explosion prevention and
                           control programs
                        •  Lack of emergency plans
                        •  Poor check on boiler and machinery
                           risks
                        •  Poor coordination of operating group
                           with other plant groups

                        •  Ineffective accident investigations
                                                                         Spills  from  processing units
                                                                         could occur

                                                                         Could result in chronic
                                                                         piping  leaks
                                                                         Could  result  in spills at
                                                                         loading/unloading areas
•  Can lead  to  open valves,
   unwanted  discharges etc.
                                                                      •  Unexpected spills  are common
                                                                         in start-up and  shut-down
                                                                      •  Spill control plan  lacking
   All equipment  failure factors
   which can result  in fires can
   result in spills
                                                                         Operations may not  have been
                                                                         given responsibility  for
                                                                         factors which could cause
                                                                         spills
                                                                         Spill prevention must be
                                                                         integral part of plant
                                                                         operations
                                               38

-------
Standards for mechanical, electrical, fabrication, chemical and performance
can be found among the societies shown in Table 9 to meet virtually any
desired specification.  These vary from standards such as nominal diameter,
material, and type of connection for small diameter piping to detailed
codes for the manufacture of pressure vessels subjected to independent
certification.  Our literature survey of equipment and design criteria con-
firmed the availability of types of equipment, materials of construction,
design criteria, and manufacturing standards to achieve the construction
of high integrity liquid handling systems.  Consequently, the major efforts
of our literature search were devoted to determining what spill prevention
procedures existed.

     The most pertinent literature references for spill prevention and
control through specified operational procedures are based on controlling
substances classified as hazardous because of the potential for fires and
explosions or because of human toxicity.  Safety in the petroleum and
chemical industries has received the most attention by organizations such
as the American Petroleum Institute, Manufacturing Chemists Association,
Underwriters Laboratories, American Insurance Association, and the National
Fire Protection Association.  Technical publication of these organizations
are oriented toward procedures and standards for equipment manufacture,
installation and operation for preventing fires and explosions and for
providing  for personnel safety and minimizing property damage.  These
reports  and studies present both detailed and broad general guidelines
and specific procedures for fire protection.  Typical examples of the
subjects covered are shown in Table 10.  None of these procedures and
standards  are directed toward spill prevention from the viewpoint of
environmental protection; however, many of these jfire and hazards pre-
vention procedures will indeed prevent spill :pollution incidents.  The
following  is an example of a typical codet^lJwhich has applicability to
prevention of pollution by oil and hazardous materials.

      "Drainage and Diked Areas:  The area surrounding a tank
     or  a  group of tanks shall be provided with drainage as
      in  Paragraph 2172, or shall be diked as provided in
     Paragraph 2173, to prevent accidental discharge of
     liquid from endangering adjoining property or reaching
     waterways, except that in particular installations these
     provisions may be waived or altered at the discretion of
     the authority having jurisdiction when the tanks under
     consideration do not constitute a hazard to adjoining
     property."

     "...The drainage system shall terminate in vacant land or
     other area or in an impounding basin having a capacity
     not smaller than that of the largest tank served.  This
     termination area and the route of the drainage system
     shall be so located that, if the flammable or combustible
     liquids in the drainage system are ignited, the fire will
     not seriously expose tanks or adjoining property."
                                    39

-------
                        TABLE 9
  PROFESSIONAL GROUPS ESTABLISHING EQUIPMENT AND
FABRICATION STANDARDS PERTINENT TO SPILL PREVENTION
    American Petroleum Institute

    American Society of Mechanical Engineers

    American Society for Testing and Materials

    U. S. A. Standards Institute

    American Water Works Association

    American Iron and Steel Institute

    American Welding Society

    Association of American Railroads

    Valve Manufactures Association

    Welding Steel Tube, Institute

    Manufacturers Standardizations Society of the Valve
      and Fittings Industry

    National Association of Pipe Nipple Manufacturers,
      Inc.

    National Certified Pipe Welding Bureau

    Pipe Fabrication Institute

    Tubular Exchanger Manufacturers Association

    Manufacturing Chemists Association

    Society of Automotive Engineers

    Hydraulic Institute
                             40

-------
                               TABLE 10

                 TYPICAL PUBLICATIONS ON HANDLING
                FLAMMABLE AND ITAZARDOUS MATERIALS
  SPONSORING ORGANIZATION
American Petroleum Institute
American Petroleum Institute
American Petroleum Institute
American Petroleum Institute
Manufacturing Chemists
  Association

Underwriters' Laboratories
  Standards for Safety

Underwriters' Laboratories  •-'
  Standards for Safety

National Fire Protection    i  s
  Association

American Insurance Association
American Insurance Association
American Insurance Association
National Board of Fire
  Underwriters
National  Board  of  Fire
   Underwriters

American  Petroleum Institute
American  Petroleum Institute
               TITLE

Recommended Practice for Cleaning
Petroleum Storage Tanks

Recommended Practice for Cleaning
Tank Vehicles Used for Transportation
of Flammable Materials

Guide for the Storage and Loading of
Heavy Oil, Including Asphalt

Practices for Bulk Liquid Loss
Control in Terminals and Depots
(covers evaporated losses)

MCA Cargo Information Card—Manual
for Bulk Dangerous Cargoes

Hose for Conducting Gasoline
Steel Underground Tanks for Flammable
and Combustible Liquids

National Fire Codes, Volume I,
Flammable Liquids

Highway Transportation of Extra-
Hazardous Commodities

Liquefied Petroleum Gas, Safe
Handling and Use

Supervisor's Safety Memo, Emergency
Planning; and Supervisor's Safety
Memo, Accident Prevention

Processes, Hazards and Protection
Involved in the Manufacture of
Spirituous Liquors

Fire  Hazards and  Safeguards for the
Metal Working Industries

Safe  Maintenance  Practices in
Refineries

Tank  Vehicle Bottom Loading and
Unloading
                                  41

-------
     "...Where  provision is made for draining water  from
     diked  areas, drainage shall be provided at  a  uniform
     slope  of not less  than one per cent away from tanks
     toward a sump,  drainbox or other safe means of
     disposal located at the greatest practical  distance
     from the tank.  Such drains shall normally  be con-
     trolled in a manner so as to prevent flammable  or
     combustible liquids from entering natural water
     courses, public sewers, or public drains, if  their
     presence would  constitute a hazard.  Control  of
     drainage shall  be  accessible under fire conditions."
     "Piping systems shall contain a sufficient  number  of
     valves to  operate  the system properly and to  protect
     the plant. Piping systems in connection with pumps
     shall contain a sufficient number of valves to  control
     properly the flow  of liquid in normal operation and in
     the event  of physical damage.  Each connection  to  pipe
     lines, by  which equipment such as tank cars or  tank
     vehicles discharge liquids by means of pumps  into
     storage tanks,  shall be provided with a check valve
     for automatic protection against back-flow  if the
     piping arrangement is such that back-flow from  the
     system is  possible."

The literature  on procedures for detection, prevention  and control of
spills is primarily  focused on oil and petroleum products.  These pro-
cedures are most often  incorporated in rules and regulations,  such as
reviewed in Chapter  III, or in publications of professional  societies
dealing with the control of waste water influence  from  industry.   For
example, a report by the American Society of Lubrication Engineers £22]
defines the oily-waste  control program and methods for  evaluating the
quality of the  program. It discusses control of oily waste  generation
at the source  and presents general procedures for  prevention and  control
of oily-waste  pollution.   Two examples of problems and  solutions  have
been condensed  into  Table  II.  The overall picture that developed from
our literature  surveys  showed that most procedures for  spill prevention
and control programs must  be based on design criteria,  engineering
judgment, facility  construction and good housekeeping procedures.  An
increasing need to  step back and  take an  "unbiased view" of  the operations
from a number  of viewpoints such  as pollution potential in case of fires,
power failures, flooding or other natural disasters, sabotage, operator
inattention  and so  on, has resulted  in a check  list such as given in
Table 12.123j   An  example  of a  simple safety check list for  heater
operations, transport  and  storage in  the  chemical  and allied industries
is shown in Table  13,  taken  from  a hazard survey 120] by the  American
Insurance Association.   It is apparent  that a system designed to be "fail-
safe" will be  less  prone  to pollution causing incidents when spills of
hazardous materials  occur  under  less  severe circumstances.
                                   42

-------
                              TABI.K  11

      CASE STC1JY laVlfLUS  OF  PKOCKDrlll.S  1'CS OVKKCOMKW Oi!. POLLUTION



                                                  soLmoss
Petrochemical plant  located on
Gulf Coast Bay v,is dlnrhitrglng
excessive aniounlb of oil  In
waste vati>r stream.  All  plant
effluent passuJ through 
-------
                                    TABLE 12

                   TYPICAL CHECKLIST FOR PROCESS EXAMINATION


FOR THE OVERALL PROCESS

1.  List all highly toxic  materials  used  or  formed in the  process.   For each
    material:

         •  List the conditions  necessary for  it to be reJ.eased  to  the
            atmosphere  or  to  surface or underground waters.   (Does  it
            normally occur in the  process as a vapor, as a highly volatile
            liquid, as  a nonvolatile liquid, or as a solid?   If  it  Is not
            easily vaporized, what process conditions could  cause it to be
            sprayed into the  atmosphere as a liquid aerosol  or dust cloud?)

         •  List the time-concentration levels in the atmosphere that will
            produce an  effect on human health.  List the exposure level in
            water as a  function  of event  duration at which toxic effects
            to marine life and to  human health become apparent.   Are the
            toxic effects  reversible or permanant?

2.  For all materials used or produced in the  process and  other  nearby processes,
    consider chemical reactions  that could take place in the atmosphere or in
    sewers and streams  between possible chemical species to  produce other, highly
    toxic materials not present  in the process.  For any such compounds that
    could be produced,  list the  same information as for Item 1 above.


FOR CONSIDERATION OF INDIVIDUAL  PROCESS ITEMS  REQUIRING DETAILED STUDY
1.  List those pieces of  equipment  containing sufficient  toxic  material to
    produce a hazard if their contents  were  suddenly released to  the environment.

2.  List those items that could produce hazardous quantities of toxic material
    through interaction if the contents of two vessels were released simultaneously.

3.  List equipment containing design  elements likely to leak hazardous materials
    such as pump packing, tank vcr.ts — or leaks that might be caused by corrosion
    of equipment, etc.  For each item listed, indicate what safeguard has been
    taken to prevent normal leakage,  such as packless pumps, double rotary seals,
    vents connected to a scrubber,  etc.  Is each safeguard adequate and reliable?


DETAILED STUDY

For each item retained on a list under  the individual process items, consider the
following:

1.  For each process vessel:

         •  What are the utilities  required? What  could  happen if
            one of these, utilities  were suddenly  and permanently
            interrupted?   If  temporarily interrupted?
            What would happen if tnc flow of one or morc Qf
            process streams cutting or leaving the vessel were
            interrupted?  What if it were twice the desired
            quantity?  W.iat would happen if the. normal outlet
            connections from the vessel became plugged?
                                    44

-------
                        TABLE 12 (Continued)


         •  Is the collection efficiency adequate to prevent hazardous
            conditions under normal operating conditions?   What
            abnormal plant conditions can impose the greatest load
            on this equipment?  For how long is it possible for these
            abnormal conditions  to  persist?  What would be the collection
            efficiency under these  conditions of increased or decreased
            flow?  Would it be adequate?

         •  What would happen in case of utility failure or flow
            stoppage (loss of motive force
            collection device?

         •  What would happen to the collection device if  surrounded
            by fire?  Could it suffer an internal fire?  What then?

         •  What can happen on collection-
            malfunction?

         •  In case of  a small leak caused  by  corrosion, what
            would happed to  the  leaking  material?  Would it
            produce an  environmental hazard?   How  long might
            it leak before being detected?  Would  the leak hasten
            the corrosion  and failure of the vessel?

         •  In case of  failure of the vessel,  how  would  the
            content be  contained?   If volatile, what would be
            done to prevent  its  vaporization?

         •  What would  be  the effect of  overpressure?   If
            protected by overpressure release devices,  how
            would the materials  released be contained?   What
            would be the effect  of  overheating?  Of  overcooling?
            Could the vessel be  surrounded  by  flames  from burning
            material released because of failure of  other equipment
            in the area'!  If so, what would happen if the fire
            lasted for  many  hours?

         •  What would  be  the effect on  vessel and contents  from
            sudden plant flooding,  violent  storms, or earthquake?

         •  What operator  error  or  instrument  failure could  en-
            danger the  loss  of vessel contents?

2.   For instrumentation on equipment that handles  hazardous  materials:

         •  What would  happen upon  power or motive force failure
            to one instrument,  or a group of instruments?   To
            all instruments?  What  position would  control  valves
            seek?  Is this the best position to minimize hazards?

         •  For each instrument, what can happen in  case of  sensor
            failure?  In case of control valve seizing? Would the
            operator receive warning in  time to take corrective
            action? Should it be clear  to a poorly trained  operator
            what corrective action  is needed,  or can the situation
            be handled with built-in automatic overrides?

3.   For material-collection, containment or pollution-prevention equipment
    (scrubbers, dust collectors, condensers,  flares,  combustion incinerators,  etc.);
                                   45

-------
                          TABLE  13

            .CHECK, USX FOR HEATER,  COMMON TRANSPORT

                    AND STORAGE  OPERATIONS
1.   Have the potential hazards of all materials involved been
    evaluated?

2.   Are precautionary measures taken to guard against acci-
    dental release of flammable or toxic liquids,  gases or
    combustible dusts?

3.   Are unstable chemicals handled in such a way as to mini-
    mize exposure to heat, pressure, shock or friction?

4.   Are the unit operation facilities properly designed,
    instrumented and controlled to minimize losses?

5.   Have all heat transfer operations been properly evaluated
    for hazards.

6.   Have all transport operations been checked for operator
    safety?

7.   Are shipments of chemicals from the plant packaged,
    labeled and transported in accordance with current regu-
    lations?

8.   Are waste disposal and air pollution problems  handled in
    accordance with current regulations?
                             46

-------
From this survey we conclude that the most detailed design criteria,
equipment specifications, and operational procedures are for either unusual
operating conditions, e.g., temperatures and pressures significantly
above or below ambient, or where hazards to property and personnel are
high such as from fire or toxicity.
C.   INDUSTRIAL UTILIZATION OF  SPILL PREVENTION AND CONTROL TECHNIQUES
     Literature  sources provided no basis  for  establishing the fre-
 quency with which  industry  utilizes available  techniques  for prevention
 and  control of spills  in  its handling  of hazardous  substances.  The only
 spill control technique that could be  ascertained as  used with high fre-
 quency is  dikes  around tanks holding flammable materials.  However,
 the  usage  of dikes is  primarily  to meet  fire and safety regulations.
 Consequently, it was  concluded that the  type and frequency of industrial
 utilization of spill  prevention  and control equipment and techniques
 would have to be developed  from  plant  inspections.
                                     47

-------
                            V.  FIELD SURVEY
A,   METHODOLOGY
     For our field surveys we selected  facilities  to obtain a cross-
section of geographical locations and types  of processing industries.
We included large integrated plants with  continuous operations,  for example,
petroleum refineries; plants handling small  volumes of hazardous polluting
substances, for example metal plating;  and plants  handling a multiplicity
of substances.  In other studies we had developed  inventories of major
transport, transfer, and storage facilities  for hazardous polluting sub-
stances at four geographical locations  in the United States:  Texas City,
Texas; Baltimore, Maryland; Charleston, West Virginia; and San Pablo Bay
and Suison Bay, California.f24,25]  Inasmuch as these areas had been
surveyed rather thoroughly, we  selected additional sites to survey
practices and procedures in order to complement the earlier work:  Nex^r
York - New Jersey, Houston, Texas, Los  Angeles and San Francisco, and
Illinois - Michigan.

     Using our experience  in process design  and project management and
the experience of our past  surveys, we  established an outline of the
pertinent questions  to  ask  and  the types  of  observations to be made.
 (See Appendix E.)  We also  discussed with process  design and construction
companies  (architect-engineering firms) the  spill  control procedures they
incorporate  in their designs.   We visited a  number of local and  state
regulatory groups, as well  as  the Environmental Protection Agency Regional
staff, and discussed the need  for additional regulations as envisioned  by
these  groups.

     In our  survey and  discussion program we contacted 37 companies and
organizations.  At many of  the  individual facilities, we observed several
different operations or manufacturing processes;  for example, bulk oil
storage and  distribution was  often a part of an oil refinery storage and
complex at which  site petrochemicals were also being manufactured.  The
surveyed  facilities  cannot  be  separated easily  into concise categories
because of the complexity  of  the process  operations, the number  of loca-
tions  at which hazardous  polluting substances were handled, and  the number
of  these  substances. Consequently, we  have  listed the number of facilities
and groups under  eight  general  categories (Table  14).  However,  the total
is  greater than the  number of  visits because of the multiple operations
that were often found.

     As we visited the  plants  and  analyzed  and  compiled  the data obtained,
 it  became clear that the  results  could  be presented and  summarized in
at  least  three ways: by  type  of  industry;  by  type of prevention approach—
design criteria,  procedures,  equipment, etc.;  and by  "unit  operations"—
storage,  transfer processing,  etc.   Of  the  three,  we selected  the  last.
The first method  would  present  information  from only a  few  sources thought
to  be  representative of large  industrial  sectors.   It  could  easily lead
                                    49

-------
                                                   TAW.K 14
                         I'Aai.rnrs,  ACKNCIKS AND OUCANI/ATION:; vismn IN nn.n SURVEY

                                           Bulk
                                            Oil      Oil
Plant
                                          Storage  Refinery                                                       UeslRners
                                            and     Storage                       Rubber                             and
                                          Distri-     and     Petro-                or        Metal  Regulatory      Con-
                                          bution   Complex   QirMnlcjl  Chemical  Plastics   Products  Agencies    structors

                                                                                                                      Y
Badp.cr Company, Inc.
StoiH' ami Webster Lngincerlng Corp.
The Lummus Company
Fluor Corporation
Bechtel Corporation                                                                                                   X
Texas Water QualHy Board                                                                                 x
Trx;is Railroad Commission                                                                                 x
California State iJalcr Control Board                                                                      x
California Fish & C^rae                                                                                    x
EPA— F.dison Lab                                                                                           x
EPA--Pacific Divlsic-n                                                                                     x
Louisiana Wildlife i Fisheries Cora.                                                                       x
Metropolitan San. Ulst. of Chicago                                                                        x
Coodyoar Chemical Company                                                  X         X
Ethyl Corporation                                                X         X
Atlantic Richfield Ompany                   XX          X
Shell Chemical Company                                           X         X
Mobil Oil Corporntic.i                        X        X
General Motors Corpr-ration                                                                      X
Dow Chemical Company                                                       X
Union Oil Company                            X        X
Proctor and Gamble Company                                                 X
U. S. Steel Corporation                                                                         X
General American Transportation Corp.        X
Standard Oil Company of California           X  .     X          X
Hercules, Inc.                                                             X
Curliss-WrJght Corporation                                                                      X
Amcrad.1 Hess Corporation                     X        X
Humble Oil and Refining Company (2 loca-     XX          X
Humble Oil and Refining Company  tlons)      X        X
Stauffer Chemical Company                                                  X
The  Upjohn Company                                                         X
Enjay Chemical Company                                           XXX
U. S. Industrial Chemicals Company                                         X
Olin Corporation—Agricultural Division                                    X
Du Pont Company                                                  X         X
     TOTAL                                   87          7        12         238          5
                                                          50

-------
to repetition because many prevention methods are similar throughout
Industry.  In the second, we would  fare the  Inherent dirfieultv of trying
to decide whether a "prevention practice"  is a design criterion, equipment,
or a procedure.  For example, is the use of  a dike with a closed drain
valve around an oil tank a design criterion  or an example of equipment;
is the practice of closing the valve an operational procedure?

     We found that the industrial facilities we visited could be readily
classified into unit operations:  storage, transfer, loading and unloading,
processing, and waste treatment.  Each type  of unit operation has basic
elements or spill prevention techniques regardless of the type of facility
or products handled.  Thus we have  summarized the results of our surveys
in terms of these operations even though the details of practices used
at each facility were expected to differ.  Finally we have combined the
results of this survey with those obtained in earlier investigations to
obtain a better overview of the spill prevention measures presently used
by industry.
 B.   SURVEY RESULTS
     The  results  of  the  field  survey  are  presented  in a series of tables
 given  in  Appendix F.   Each  table  in Appendix  F  lists the major design
 criteria, operating  procedures, and equipment used  at each facility for
 the prevention  of spills of oil and other hazardous materials.  In some
 facilities,  it  was not difficult  to determine the principal practices
 used;  in  others,  the concern of the plant management for outside visitors
 or the proprietary nature of the  operations may have prevented full dis-
 closure of  all  the measures used.  Also,  we found that in some facilities
 equipment and procedures which could  be used  to prevent spills were con-
 sidered routine and  not  specifically  mentioned  by the facility personnel.
 Thus,  these tables are not  totally complete.  Of course, one would expect
 a considerable  variation of methods and equipment because of the diversity
 of types, locations, ages of the  facilities visited, and the different
 processes and hazardous  materials used.

     In order to  make a  more comprehensive presentation of the results of
 the plant visits, we have summarized  in tabular form the principal design
 criteria, equipment, and procedures we observed in  each operational area—
 storage,  transfer, loading  and unloading, processing and waste treatment.
 The tables  show the  number  of  facilities  in which we observed each practice;
 this provides an  indication of the acceptance of this practice by industry.
 The number  should not be regarded as  precise, but shows the relative use
 of the different  practices. A brief  discussion of  the practices is also
 given. Another table is given to summarize "management procedures" which
 plant  management  personnel  thought were effective in preventing spills of
 oil and hazardous materials.
                                    51

-------
1.    Storage

     Table 15 summarizes the major practices for spill prevention In
storage areas.  In addition to these,  at  least  one facility used each of
the following practices:

     •  Log of condition of valves on  all tanks and dikes
     •  Impermeable membranes around tanks
     •  No bottom pipe connections in  tanks
        (load and unload from top entry pipes)
     •  Gravity loading of tanks

We note that none of these procedures  is  fail safe by itself;  a combin-
ation of design criteria, procedures and  equipment is required.

     a.   Spill Prevention

          Because storage tanks have a very long service life, most
          facility operators inspect tanks for corrosion and weakening by
          nondestructive and destructive  testing methods.  Visual inspec-
          tion from the outside of the tank is often coupled with other
          routine maintenance, such as painting, but unfortunately is
          not regularly scheduled in most facilities.  Ultrasonics is a
          good, but very time consuming and tedious means of determining
          the wall thickness of a tank non-destructively.  This method is
          applicable to an empty or filled tank but normally is used for
          spot checks rather than to scan the entire area of the tank.

          Although diligent inspection can prevent a corrosion-induced
          tank rupture, a tank may fail because of the pressure differential
          created between the inside and outside when the tank is emptying
          and the vent becomes clogged.  This kind of catastrophic spill
          event can be prevented by simple maintenance and inspection of
          vents and vent lines on storage tanks, to insure that they are
          open, and also by monitoring pressure in the vapor space at the
          top of these  tanks.  The vapor space pressure was not measured
          in  any of the facilities we visited; however, a low pressure
          alarm system  could prevent the occurrence of this infrequent,
          but catastrophic spill event.

          Spills resulting from overfilling a tank can be avoided with a
          gauging system that displays or indicates the instantaneous
          liquid level  in the tank—such information is acted upon by the
          personnel charged with controlling the operations of the storage
          facility.  However, these types of level indicators and associated
          transmission  and read-out instrumentation were found not to be
          used frequently because of malfunctions.  A more universal pro-
          cedure was for plant personnel once each day to measure the
          liquid level  in each tank by means of a dipstick.  Plant opera-
          tors believe  this kind of activity not only prevents accidental
                                    52

-------
                PRACTICE

Dikes, fire walls,  or earthen
barriers around tanks


Drainage ditches and graded
surfaces surrounding tanks

Manual gauging of storage tanks
at regular intervals
Separate drainage
diked tanks
                  >,vstem for
Planned inspection o£ all tanks,
dikes and equipment in storage
area at regular ±nfervals
Automatic level garging in
tanks; or gauging manifolds
Automatic high and low level
alarms (or pressure alarms) for
storage tanks

Specified procedures for removal
of rain water from diked areas
 Locked or sealed valves on drain
 lines in diked areas

 No drain lines in diked area;
 sumps and pump out systems used

 Equipment (trucks) available
 (mandatory) during tank cleaning

 Written procedures followed in
 transferring to or from all
 storage tanks

 Spare tanks or catch basins
 specifically designated for e
 storage tank

 Specific overflow lines from
 storage tanks to sumps or catch
 basins with alarms
 Tank contents analysed before
 transfer
                                                   TABLE 15

                                      Sl'MMARY OF SPI1.I. PRFVKOTION PRACTICES

                                               IN STORAGE AREAS
    TYPE

Design criteria,
equipment
                      NUMBER OF
                      FACILITIES*
21
Design criteria            7


Procedure                  7


Design criteria            6




Procedure                  5
Equipment

Equipment


Procedure



Procedure

Design criteria
equipment

Equipment
Procedure

Procedure

Procedure
Design Criteria


Design Criteria
Equipment



Procedure
                REMARKS

Usually required by fire codes; may
be used only for flammable or hazardous
materials

Ditches may be part of the storra water
sewer or process sewer systems

Dip sticks used as positive level
measure; often prior to and after transfer
Any spills in and around diked area can
be diverted to retention ponds or other
facilities without overloading waste
treatment facilities

Frequently a written inspection plan
by maintenance staff to examine area
for potential failure points
Measurement system to display tank
contents to operator in central location

Most alarms indicated in central control
rooms or supervisory locations which
are manned 24 hours/day

Insures that dike valves are normally
closed and prevents spills from emptying
Into vaste treatment stream

Prevents spills from leaving diked area

Both rainwater and spilled material must
be pumped to treatment area

Prevent release of sludge or waste, and
reduce waste runoff during next rain
Other facilities had procedures for
special situations or materials

These could be used in emergency
situations

Provides both indication of overfilled
tank and prevents loss of material

Basically a safety measure to prevent
mixing hazardous materials and loss
of product quality
 * A  total of 23 facilities were visited.
                                                      53

-------
     overfill  but  also  helps  to  detect  a  leak  which might  go unnoticed
     during the  normal  routine.   The  measurement  also detects errors
     in or malfunctioning  of  instrumentation and  control equipment
     used to operate  the tank farm facility.   Level alarms on tanks
     were not  observed  often  in  our survey,  apparently because of
     questionable  reliability of these  systems.   Two of the five
     architect-engineer firms we visited  recommended automatic
     gauging or  alarms.

     Storage tanks used for crude petroleum  and certain other
     organic intermediate  and refined products collect a heavy thick
     sludge on the tank floor and must  be drained periodically and
     cleaned.   Several  facilities we  visited have well established
     procedures  for the cleaning process, including the use of vacuum
     trucks for  removal and precautions to insure that any excess
     spilled material will remain in  the  diked area or be treated
     effectively in a waste handling  system.

b.   Spill Detection

     The only effective way of detecting  spills in storage tank
     areas reported in  our survey is  planned visual inspection by
     the operating personnel  frequenting  the area.  Discussions with
     architect-engineering firms, and with several companies in the
     chemical processing industries indicate that good design in
     storage tank farm  facilities includes the strategic location
     of one or more instruments  or controls  which require the
     periodic checking  and data  recording by plant personnel.  These
     controls are deliberately located  in such a  way that plant
     personnel must periodically traverse the  storage tank farm area
     and thus help insure  rapid  visual  detection  of leaks.  This is
     a good example of  current state  of the  art,  where good design
     practice is short  of  total  automatic data acquisition and
     transmittal and process  control, and where the human element
     deliberately included as a "fail-safe"  aspect.

     The larger and more modern storage tank farm facilities are now
     being designed with sensing devices such  as  liquid-level
     detectors in all of the  tanks, with data  transmission systems
     connected to a central control room. A computer can keep track
     of an instantaneous inventory and material balance and show any
     spill of sizable proportions as  an unaccountable loss.  Although
     the computer system is used primarily for inventory control, the
     potential for spill detection is inherent in the system.  One of
     the facilities we  visited was in the process of installing such
     a system.  Another plant was considering  the use of closed circuit
     T.V. to help detect spills  in storage areas.
                              54

-------
c.  Spill Control

     Insurance, safety, and  fire codes  typically require that above-
     ground storage tanks used  for  flammable  liquids be surrounded
     by a fire wall or dike  sufficiently high (with some maximum height
     normally specified) to  contain at  least  100% of the maximum
     storable or usable tank volume.  Fortunately these dikes also
     provide the primary means  of spill control in storage areas.
     In almost all of the facilities we visited, tanks containing
     oil were diked.  Those  containing  flammable organics were also
     diked, but those containing inorganic materials were usually
     not diked, even if their contents  were hazardous.

     Dikes are usually penetrated by one or two drainage lines
     equipped with shutoff valves on the outside of the dike or
     fire wall.  These valves should normally be closed, so that
     spills and contaminated rainwater  do not flow into undesirable
     channels.  Inspection,  valve locks, seals and other means were
     used in several facilities to  assure this does not happen.
     Another approach used  in a few small facilities was a sump
     and pump operation  to  drain dikes, thus  precluding gravity flow
     of spilled material.   After a  heavy rainfall, plant personnel
     normally inspect the rainwater contained in each dike for
     evidence of contamination.  Several facilities had detailed
     procedures for  sequentially discharging  rainwater after inspection.
     In most  facilities,  if the water  appeared clean it was sent
     directly  to clean-water discharge  from the plant.  In several
     facilities, the discharge  from diked areas was routinely sent to
     the waste  treatment  facility,  a more conservative and fail-safe
     approach.

     Dikes  or  fire walls  can be very effective means for controlling
     small  spills or leaks  from storage tanks. However, the normal
     dikes  or  fire walls  used today have been totally ineffective in
     containing some major  and  catastrophic leaks  from large storage
     tanks  which  resulted in the generation of a large high-velocity
     jet  of liquid  issuing  from the side wall of the tank.  Such
     spills have been known to  rapidly wash out a  dike at which it
     was  directed and  render the dike  ineffective.  Also the high level
     of kinetic energy  associated with a  large jet  of liquid issuing
     from the  side  of  a storage tank has been known to cause a jet
     of liquid  to simply wash over  the top  of a dike, since dikes
     are  designed to  restrain and  confine  a  gradually deepening pool
     of  liquid  rather  than  a stream of liquid moving a high velocity.
     Evidence  is now accumulating that dikes  require more  engineering
     consideration  due  to their failure to withstand shock loading.
     Reinforcement  and  overhang design should aid  in  controlling  dike
     failures.
                               55

-------
          A backup  control  system  found  In  about  one1-fourth  of  tin1
          faculties  we  visited  was  to u.se  drainage  ditches  around the
          storage area which  were  either  (1)  separate  from the  remainder
          of the plant or  (2) formed a part of  the chemical  waste disposal
          system.   Thus  any leaks  from the  storage area,  or  leaks through
          valves in dikes,  would be  conveyed  to a waste treatment facility
          rather than discharged with storm water.

2.    Transfer

     Table 16 summarizes the  major practices  for  spill prevention in the
transfer process.   (As noted  in  the  Introduction, we have defined transfer
as the piping between storage and  process areas,  and related pumps, etc.
Other practices are given later  which are more  specific to loading and
unloading areas.)   In addition to  these,  one  or two  facilities  used the
following:

     *  Flange bonnets on all pipeline  flanges
     to  Samples analyzed prior to  transfer  in line
     f>  Planned attempt  to reduce  the number  of flanges in pipelines
     •  Low pressure  shut off in pipelines

Two of the architect-engineering firms visited  recommended above grade
piping throughout  the plant with appropriate  drainage  system underneath.
All of the architect-engineering firms visited  recommended welded piping
systems for both process and  transfer areas to  help reduce leaks from
flanges.

     a.   Spill Prevention

          Management  personnel of  the facilities we visited indicated that
          preventive maintenance is  a necessary and most effective means
          of preventing spills from failure of  pipes,  pumps, valves, and
          other components.  The proximity  of a large number of pipelines
          running a parallel  course on common supporting structures
          greatly facilitates routine painting  and inspection programs.
          Surveillance by plant personnel is generally intensified on
          those pipe transfer systems whose color code indicates that
          they carry the more hazardous  liquids.  Therefore, the visual
          examination of pipelines is probably  increased in direct propor-
          tion to the hazard of the liquid being transferred.  Another
          form of preventive maintenance found useful to some plant
          operators is routine inspection and periodic replacement of com-
          ponents which past  operating practice has indicated have a limited
          service life—for example, valve seals and shaft seals on pumps,
          which wear out with a rather predictable frequency.  Use of
          welded pipe joints  rather than flanges helps eliminate part of
          this problem.
                                   56

-------
                                                  TAB1.K  1(>

                                     SUMMARY OF SIM I.I. I'KI-VliNTION PRACTICES

                                               IN TRANS]-ER ARK\K
                PRACTICE                  TYPE

Planned periodic inspection of all
pipelines, combined with preventive   Procedure
maintenance

All pipelines located above- grade
to facilitate inspection and Idonli-  Design criteria
flcation of leaks

Concrete ditcher »:nder pipelines,
lead to chemical vaste system or      Design criteria
waste water syr.ttr;,

Vlant procedures require operators
to walk pipelines on daily basis  for  Procedure
inspection

Pressure relief valves in portions
of pipeline                           Equipment


Written procedures  for pipeline
transfer                              Procedure


Leak detection  n>rtcr. usinR
computer monitored  flow meters and    Equipment
tank level  indicators
Check valves  and storage  tanks
at ends of  pipelines specifically    Equipment
for spill prevention and  control

Cathodic  protection system for
underground pipelines                 Design  criteria


*A total  of 23  facilities were visited
NUMBER OF
FACILITIES*
                                  REMARKS

                  Most inspections include some hydro-
                  static pressure tests or ultrasonic
                  tests

                  Generally found in newer facilities
                  In mcst cases,  these act to drain plant
                  area as well as conduct any spills to
                  treatment area

                  Strategic placement of valves, meters,
                  etc. require operator to survey pipeline


                  These were not fail-safe measures in
                  themselves, but valve opened to channel
                  which led to waste treatment facility

                  Also, telephone procedures for several
                  plants with long pipelines or inter-
                  plant pipelines
                  These systems were found in large
                  refinery operations
                  Most likely oiany facilities used cathodic
                  protection but only 2 indicated that it
                  vas a spill prevention measure
                                                         57

-------
     Another prevention practice we observed in several facilities
     is the use of seals on valve handles which normally should remain
     in some particular position.  Any movement of the valve handle
     breaks the seal and alerts operating and maintenance personnel
     that the valve is no longer in the desired position.

     Several plants use written procedures for transfer of fluids by
     pipeline.  This practice seems to be becoming more standard.

b.   Spill Detection

     Simple visual inspection is the most commonly used means of
     detecting spills associated with transfer of liquids.  Plant
     personnel frequently travel along and under the pipe racks.
     Pipeways are often laid out not only so personnel can easily
     inspect them but also so personnel must frequently pass the
     pipeways on their way to perform other unrelated tasks.  This
     practice increases the exposure of plant personnel to the
     actual physical transfer pipeline facilities.

     Unfortunately, newer and highly automated production plants
     are designed to be staffed by a minimum of personnel.  It is
     not uncommon for a large, highly automated chemical plant to be
     operated by five to ten operating personnel who spend a large
     part of their time in a central control room.  Therefore, an
     accidental event such as the rupture of a pipeline might be
     detectable only through data transmitted to and displayed within
     the control room—drop in pressure or a change in flow rate for
     example.  Only a few of the plants we visited had enough monitor-
     ing equipment for routine detection of pipeline spills from
     control rooms.

     Classical inventory control permits detection of spills in some
     plants.  The more refined, accurate, and frequent the inventory
     balances, the more quickly a spill can be detected, and the more
     sensitive the technique is to detecting even smaller spills.
     The availability of large and effective digital computer systems
     to industry has made possible the means for maintaining almost
     continuous and very close surveillance of the flow rates of
     liquid into and out of all the active pipelines at a large
     chemical-processing plant.  Two of the plants we visited have
     installed such systems, several others were considering
     developing this kind of system capability.  The primary purpose
     for this kind of inventory control system is to optimize the
     utilization of production facilities and the scheduling and
     movement of liquids and various bulk carriers to and from  the
     plant.  A direct "spin-off" of this kind of monitoring and
     surveillance  system, however, is the potential for detection
     of spills.
                              58

-------
         A simple, yet apparently  effective, approach  that we found used
         in several plants and  considered  in others  is a pressure-sensing
         device and associated  system  to actuate  automatic valves and seal
         the pipeline at  strategic points  to minimize  Hie  total spill.

    c.   Spill Control

         In addition  to  the  strategic  location of manual or  automatically
         actuated valves  along  pipelines,  the  most commonly  accepted
         practice for control of  spills from piping  is to  place a concrete
         or hard surface  ditch  under pipeline  racks.   The  ditches normally
         drain rainwater  to  storm water disposal  systems,  but are usually
         arranged so  that a  spill from a pipeline, once detected, can be
         diverted to  a  chemical or oil waste disposal  system or an impounding
         area.  In  locations where ditches or  gutters  are  not suitable,
         graded hard  surfaced areas are frequently used to direct any
         spilled material into  chemical or storm  water sewers.  Many
         pumping areas  are curbed and  graded to help contain chronic leaks
         or spills  and  direct them to  a waste  treatment facility.


3.   Loading and Unloading

     Table 17  lists  the principal  p-ractices used at loading and unloading
areas.  In addition, the  following were used in one or more facilities.

        Cargo  sampling before loading and unloading
        Remote pump  shut  down capability
        Shut off valves upstream and downstream of pumps
        Different types of couplings for different fluids
        Gravity overflow  lines  to  sump or spare tank
        Excess flow valves (to  shut off flow if limits were exceeded)
        Routine valve check before and after loading operations

Because of the apparently high  potential for spills, and  high spill
incidence,  in loading and unloading areas,  the number of  different tech-
niques to prevent,  detect and control spills is large.  Most plant oper-
ators believe that spills are frequent during loading and unloading  because:

     1.   Each move of liquid involves one or more temporary pipe
          and/or hose connections  to be made.

     2.   This functional area  is  highly labor intensive,  and thus
          very susceptible to human error.

     3.   Loading hoses,  loading arms, and other pieces of equipment
          in this area are subject to severe use and therefore have
          a high propensity to wear and/or be damaged.
                                    59

-------
                                                  TABLE 17

                                    SIW1ARY OF SPILL PKCTKNTION PRACTICES HSKI>

                                        IN  LOADING  ASM) ('^LOADING AREAS
                                          TtVY_

Curbing, gutters,  or ditches around   Design criteria
loading and unloading areas

Collection sump with pump and/or      Design criteria,
oil separator in each loading/        Equipment
unloading area

Hard surfaced loading and             Design criteria
unloading area

Articulated swivel joint loading      Equipment
arras or rigid connectors for
loading

Loading areas sloped and graded       Design criteria
toward sumps or chemical process
sewers

Standard procedure^ for draining      Procedure
fill lines (gravity drain, bjow
back etc.)

Written procedures and check          Procedure
sheets for loading/unloading
operations

Weighing of tank cars, trucks,        Equipment,
or tanks with autot.'>.tic shut off      Procedure
at preset levels

Drip pans, scupper plugs, etc.        Equipment,
used during vessel unloading and      Procedure
loading
Neutralization tanks locally          Equipment
available for spills during loading
and unloading

Company purchased booms available     Equipment
Level jlarms on tankage used in       Equipment
loading and unloading

Seals on normally closed valves       Equipment,
nt loading site                       Procedure
Testing and certification of          Procedure
hoses at scheduled intervals

Clean up truck on site during         Equipment
loading operation
Gravity flow during loading and       Design criteria
unloading
NUMBER 0V
KAC.VUT1KS*

    11
                RKMARK_S

System used depended  on apt? oi plant
and layout of  loading/unloading area

Used with hard surfaced,  graded and
curbed loading areas.
                  Plants installing  new equipment preferrs
                  this over flexible hoses
                   Used primarily in  terminal  operations
                  Several additional plants  had written
                  procedures for materials  thought to be
                  especially hazardous

                  Meter loading of tank cars was practic
                  at two other plants

                  Only found in oil unloading operations
                  Used in facilities with  acid and caustic
                  tanks at loading sites


                   These were on site ready  to be deployed
                  Mainly for large transfer  hoses for oil

                  Oil loading only

                  Gravity flow for first half  hour or hour
                  to check for leaks
* Total number of facilities visited was 23
                                                      60

-------
     4.    There, is a high potential for poor communications between
          those on both ends of a move, for example, the terminal
          operators onshore and the crew on a vessel.

     5.    The temporary connections often are suspended directly
          over or close to waterways.  Therefore, the difficulty in
          controlling a potential spill is maximized.

     Our survey indicated that the more hazardous the nature of the
liquid being handled at the loading and unloading facility, the more
likely that various safety codes and regulations will have the indirect
benefit of reducing the spill potential.

     a.   Spill Prevention

          The most frequently used prevention measure was the increased
          use of articulated swivel joint arms at loading sites.  Plant
          operators believed that the use of metal loading arms signi-
          ficantly reduce accidents, particularly in ship and tank car
          loading.  At most of the facilities we visited, we were
          informed that new installations would use articulated arms
          rather than hoses.

          The increased use of strict written procedures for implementing
          all loading practices—such as making connections, testing for
          leaks, using gravity flow for initial loading with the second
          round of leak checks, turning the loading pumps on and making
          a third round of leak checks, draining or blowing out the
          residual liquid from the loading hoses or loading arm after
          the liquid transfer is made, etc.—was felt to be the most
          important practical method of preventing spills.  Examples of
          specific procedures are given in Appendix G.

          Good communications between the shore and any ship or vessel
          being loaded or unloaded were thought to be critical.  The
          persons in charge of the onshore facilities and the ship end
          of the transfer must be able to communicate fluently in a common
          language.

          Automatic shutoff in loading operations were not used as fre-
          quently as we expected.  Most shutoff devices consisted of an
          automatic shutoff valve actuated by a pre-set control meter or
          scale.  These were used to stop loading after the tank car or
          tank truck had been loaded to almost maximum capacity, say 95%
          of the fill.  The remaining 5% would be added manually.  Since
          only a few percent of the total fill need be monitored by an
          operator, the attention span demanded of the operator was short
          and there should be less risk of an overfill.
                                     61

-------
          Although  no I  spec I I leall v  expressed  hv  manv  operators,  we
          believe  that  prevenlntIvo  maintenance.  Inspection  of  hoses.
          valves,  pumps,  Baskets,  etc.  Is  an  Important  spill  prevention
          practice  and  shouJd  be placed  on a more rigorous schedule.

     b.    Spill  Detection

          The  principal and  almost exclusive method  of  spill detection in
          loading  and unloading is by visual observation  of  the operating
          personnel.  Rigorous requirements for operating personnel being
          present  during  all phases  of the operation is perhaps the most
          valid  method  used  today  for spill detection.

     c.    Spill  Control

          The  most common and  useful spill control measures  used  were
          curbing  or  ditches around  loading areas and  pitched,  hard sur-
          faced  areas leading  to sumps or  chemical process drains.   More
          than half of  the plants  visited  used one or more of these methods.
          Procedures  for  drainage  of lines or  blow back into vessels also
          was  used frequently.  We found that  booms  were  also used  as  a
          control  measure; they were not typically deployed  until some
          spill  had occurred.  Drip  pans and other catchment devices were
          used to  control minor leaks, but were not  used  as  a prime pre-
          ventive  or  control measure.

4.   Process Areas

     Table 18  summarizes  the major practices used in process areas. Many
of these are similar  to those  used in loading  and unloading  and storage
areas (for example, many  tanks in  process  areas are  diked).   In addition,
the following  practices were used  In one or more  facilities:

         No bottom connections on  tanks
         Overflow  lines to process sewers
         Cooling towers replace once through  process water
         Operator  on  duty 24 hours/day  in  process area
         Total elimination of  drains in  process area
         Automatic level  indicators  in  process tanks

     a.   Spill Prevention

         In addition  to the  specific prevention methods listed  in Table
         18—  primarily level alarms,  locked  valves, inspection procedures,
         elimination  of bottom connections—we found several general
         practices are  used  in the process area for  purposes other  than
         spill prevention, which plant  personnel  believe  have an important
         impact  on spill  prevention.

         1.  Equipment  design and  specification—general  adherence to
             established  construction  codes and recommended design
                                    62

-------
                                                 TABLE 18

                           SUMMARY OF SPILL PREVENTION PRACTICES USED IS PROCESS ARFAS
                                                            NUMBKR OF
           PRACTICE                       TYPE              FACILITIES*

Concrete or other hard surface        Deaiiin criteria            12
under process area

Curbing around process areas          Design criteria            11


Graded surfaces with ditches or       Design criteria            10
chemical sewers around process
areas

Separate process and storm water      Design criteria             7
sewers in process area

Sumps or holding basins  located  in    Design criteria             6
process areas

Level or pressure alarms on process   Equipment                   5
tanks

Neutralization i*nks at  Individual    Design criteria             4
process sites

Oil  skinaners oc separators at         Design criteria             4
process sites                         equipment

Separate collection  (sewer) system    Design criteria             4
for  especially hazardous materials

Monitor;' ,g  of  process waste water    Equipment                   4
for  evi  -rce of. spills at process
site
Procedures  for directing Initial     Procedure                   3
rainfall  in process  area to waste
treatment  system
Scheduled Inspection of  all process   Procedure                  3
area spill  prevention measures
Written procedures for process        Procedure                  2
operation
Sampling procedures  planned  to        Procedure                  2
minimize  spills
Locked or  sealed  valves  in process    Equipment                  3
area
            practice bv toui' »'t  i"ivo
arohitect/eny, Imvr (np, t' Inns

Recommended by all architect/engineering
firms visited
Spills must be directed to process
sewers

Fluids pumped  to waste treatment area
Specifically used for spill prevention,
not process control
Found in facilities handling large quanti*
of acids and alkalis

Reaiove oil before spilled fluid enters
waste treatment system
Aids detection of spills and spill
location
In addition to normal preventive
maintenance
Specifically mentioned as a spill
prevention measure
Saopling of process streams
 *  A total of 23 facilities were visited
                                                     63

-------
         practices  to  insure  physical  integrity  of  the  process
         system has  the  secondary  effect  of  preventing  spills.

     2.   Process control procedures  and equipment—use  of  pressure,
         temperature,  flow, level  and  composition detection and
         control systems,  planned  for  maintaining product  quality
         and controlling throughput, have a  secondary effect of
         preventing  spills.

     3.   Operational procedures—most  process  operations have written
         or carefully  planned operational procedures to maintain
         product quality and  production rate.  Such procedures  can
         and sometimes do  include  spill prevention  measures as  a
         spin off.

     4.   Preventive  maintenance—as  in other plant  areas,  preventive
         maintenance to  maintain production  can  help in elimination
         of potential  spill causes.

b-   Spill Detection

     Although visual inspection  for  spills and leaks is the most
     common method  of  spill detection, small spills and leaks—e.g.,
     from pump seals,  valve packing, flange  connections, rivets and
     seams easily go undetected.   Plant personnel admit that appro-
     priate action  is  often not  taken  to  control these  leaks.
     Unfortunately,  this usually stems from  a  lackadaisical attitude
     on the part of  operating personnel,  poor  housekeeping habits,
     and a failure  to  comprehend the possible  catastrophic effects of
     even a few pounds of some hazardous  polluting  substances on the
     aquatic environment.  The value of visual detection is increased
     greatly by a well directed  and  enforced spill  prevention program.

     Plant personnel believe  that  leaks and  spills  can  also be  detected
     by means of alarms  located  within the process  system.   The most
     valuable and most frequently  usable  in-process alarms are  based
     on instruments  that measure flow, pressure, or level  of substances
     in the process  system.   Most  of this instrumentation  is based
     on measuring and  controlling  a  dynamic  system  and  often initiates
     corrective action which  may control  or  limit the spillage.  These
     systems are most  useful  in  detecting the  likely onset of a large-
     volume spill due  to catastrophic  accidents; however,  small leaks
     and spills are  probably  not detectable  or alarmable.

     Alarms which are  independent  of the  process system are utilized
     principally to  detect materials hazardous to personnel or  property
     such as high concentrations of  hydrocarbon  vapors. These
     detectors usually initiate  a  combatant  action, such as foam
     blanketing an  area  where high concentrations of explosive
                               64

-------
          hydrocarbons are detected, or Initiating water deluges us tire
          protection.   Such action may be useful from the personnel
          hazard view but incorrect from the environmental protection
          view.

          The most common process area instrumentation for spill detection
          is installed in the process area's drainage systems,  such as
          process and storm sewers.  These include pH, hydrocarbon, TOG,
          TOD indicators.  Large maintenance costs and poor reliability
          of these instruments are the principal reason for their present
          limited use;

     c.    Spill Control

          The most commonly used methods for controlling spilled substances
          in process areas is the installation of graded hard surfaces,
          passive barriers, collecting sewers, or surface drains, which
          will prevent the substances from entering water courses.   In-
          stallation of curbed areas around processing equipment and
          catch pans and basins under areas where chronic leaks are
          expected, e.g., under pumps, is most often practiced.  Drains
          from the processing areas are generally segregated from storm
          water sewers.  Catch basins or sumps are frequently located
          within the process area.  Several plants have specific sewage
          systems for very hazardous materials, separate from other
          chemical waste and storm water.  Several facility operators
          indicated that a more formalized spill control plan for the
          process area would be the most important addition to current
          practices.

          Methods for controlling spills and leaks in a processing area
          depend greatly on the age of the facility.  In new plants,
          separate process area and land drainage sewers can be readily
          provided and are recommended by architect/engineers.   However,
          such provisions would be very expensive for old plants.  These
          costs would be analogous to the costs for separating sanitary
          and storm water sewers in many of our older cities.  Consequently,
          many older processing plants must consider alternate methods
          for the control or rapid removal of spilled substances, for
          example, providing secondary containment barriers near the points
          at which there is a high potential for spills and leaks, providing
          local sumps for spilled fluids, etc.  An alternative is to enclose
          the process area while maintaining fire and safety measures.

5.   Waste Treatment 'and Disposal

     The waste treatment and disposal system of an industrial facility
can be a spill prevention and control measure in itself.  Although we did
not examine waste treatment facilities from the view of the quality of
the effluent discharge in our field survey, we attempted to obtain
                                    65

-------
information on the methods by which the operation of the waste treatment
system help prevent spills from entering the water environment.  Table 1.9
summarizes the principal practices associated with waste treatment which
are related to spill prevention and control.  In addition, the following
practices were used at one or more facilities:

     •  Hourly inspection of oil traps and skimmers
     •  Only specific employees permitted to discharge any water
     •  Membrane liners around holding lagoons
     •  Analysis of water obtained from well points surrounding holding
        lagoons
     •  Waste treatment system operator on duty 24 hours/day

     All of the architect/engineers we visited recommended holding
lagoons, separate sewer systems in critical areas for storm water and
process waste (or spills), and effective use of a waste treatment system
as a bac'cup measure for spill prevention and control.

6.   Management Practices

     Our discussions with facility management and supervisory personnel
during the field survey revealed several types of management practices
which rfere believed to be major factors in the prevention and control
of spills.  The following practices were conducted at one or more facilities:

     •  Employee motivation program aimed at reduction of spills and
        keeping oil from entering the water
     •  Management emphasis on placing responsibility for spills on
        individual operators
     •  Educational program aimed at process unit operators to make
        them aware of the consequences of spills and that they have
        the ultimate responsibility for spill prevention
     •  Plant wide spill reporting—emergency communication system
     •  Formation of an independent pollution control group with
        broad authority
     •  Establishment of company wide pollution control education
        programs
     •  Specific training programs, with emphasis on pollution control,
        with written and oral exams to obtain operator status
     •  Random program of monitoring effluent and waste product streams
        in various parts of the process areas to alert operators to the
        need for control of chronic spills and leaks
     •  Requirement for 24 hour/day operator availability in high
        potential spill areas

     The use, effectiveness and acceptance of these practices were
influenced to a large degree by management desire to preserve water re-
sources as well as to create an acceptable public image.
                                    66

-------
                                               TABLE 19

                          WASTE TREATMENT PRACTICES WHICH AID SPILL PREVENTION
                PRACTICE

Monitoring of waste system
effluent (pH, BOD, TOD, etc) to
aid in spill det'ction
Separate sewer system for storm
water and process or trade water/
waste

Holding or diversion lagoons, ponds
or tanks for lirge spills
 Specific protic'du-e and facilities for
 diverting or treating initial
 rainfall

 Single sewer system and  treatment
 plant for all plant water—process
 runoff, etc.

 Centrally located oil separators
 and skimmers in storm water and
 process water systems
 Neutralization facilities  centrally
 located for all water systems
 Separate sewer system and  waste
 treatment facility for very
 hazardous materials
    TYPE

Equipment,
procedure


Design criteria
Design criteria



Procedure,
design criteria

Design criteria



Equipment



Design criteria

Design criteria
NUMBER OF
FACILITIES*

    12
    11
                         10
                  REMARKS

tot installed specifically for spill
detection but for effluent quality
               Hast have available methods to direct
               •pills to process waste system

               Same facilities have up to five diversion
               lagoons; others have capability of
               diverting up to one week process and
               rainwater
               May also use process and storm water
               sewers and diversion ponds

               All used water and plant effluent is
               bandied by one system

               Used  in plants which handle large
               volumes of oil
               Systems generally located at process
               areas
  A  total of  23  facilities were  visited
                                                     67

-------
C.   COMPARISON WITH OTHER SURVEYS


     In order to make the results of the present survey more useful,
and to include a larger and more diversified data base, we have re-examined
the results of several other plant surveys made in Boston, New York,
Baltimore, Charleston, W. Va.,  Texas City, Los Angeles, San Francisco,
and Houston by our staff for the Environmental Protection Agency and
others.  The facilities visited, 107 in total, varied from small repack-
aging or formulating plants handling relatively small volumes (hundreds
of gal.lons) to petroleum and petrochemical companies processing or
storing hundreds of millions of gallons.

     In summarizing observations of our survey teams, we found that a
very !<>ng list of methods, equipment, and procedures would be required
to describe all plants at all locations.  The selection of the techniques
encountered most frequently also must have a certain degree of subjectivity
based on our experiences and observations.  Furthermore, we could not be
sure tna: all methods, equipment and procedures were reported to us in
these -/ioits.  Nevertheless, we found the following spill prevention
practice:, were used most frequently.

     1,   Diked areas around storage tanks.  For flammable substances
          these are required; however, as a passive barrier to tank
          rupture, and tank and pipe connection leaks, a diked tank
          storage area is considered the first line barrier to contain-
          ing and reducing the spread of large volume spills.

     2.   Tank level indicators and alarms.  The sounding of alarms at
          prescribed levels during tank filling was expected by plant
          personnel to minimize the common occurrence of overflow
          when reliance is on manual gauging for control.

     3.   Above ground transfer lines.  Above ground installation
          permits rapid detection of pipeline failures and if used
          with hard surfaced ditches underneath, minimizes polluting
          ground waters.  Although increasing the possible mobility
          into surface waters, long term considerations are believed
          to favor above ground transfer lines.

     4.   Curbed process areas.  Spills from processing equipment must
          often be removed rapidly from the area but should be prevented
          from spreading widely in the immediate area, consequently,
          curbed areas connected to collecting sewers are used.

     5.   Area catchment basins orjlop tanks.  For containment of small
          spills and leaks in the immediate area thereby effecting removal
          at the highest concentrations, local catchment basins can
          provide significant flexibility in preventing spills from
          entering water courses.
                                    68

-------
     6>    Holding lagoons for general plant_area.  Holding lagoons, which
          can be used to segregate spills and prevent them from passing
          into wastewater treatment plant or water courses, give the
          surge capabilities necessary for handling large volume or highly
          toxic spills.

     1'    Primary wastewater treatment.  For removal of floating sub-
          stances or for the chemical neutralization or destruction of
          spilled materials, the primary wastewater treatment plants
          serve to ameliorate the more drastic effects of spills in
          receiving waters.

     8-    .Secondary wastewater treatment.  The removal of soluable sub-
          stances usually through biological action, where possible,
          can insure that the plant wastewater discharges have a high
          degree of uniformity at acceptable quality regardless of
          in-plant variations such as would occur from spills.

     9,    Availability of spill cleanup equipment.  Vacuum trucks,
          booms, neutralizing chemicals, etc. represent obvious con-
          tingency planning to cope with spills.

    10.    Routine preventative maintenance schedules.  Because literature
          sources and plant staff indicated that the cause of many fires
          and spills in the chemical industry could be traced to failures
          that might have been avoided by a thorough preventative
          maintenance program, it was recognized that this program could
          be an indicator of the possible reduction in spill potential.

    11.    Spill control plan.  The formalization of a plan for coping
          with spills and the training of personnel in courses of
          action similar to plant safety programs, was reasoned to be
          a prime indicator of the operational possibility of coping
          with spills in a manner which would avoid entry into water
          courses.

     Using the prevention factors outlined above, we have tabulated the
results of 107 plant surveys.  In this total number there were 31 plants
which we categorized as chemical plants.  The remaining 76 plants included
a broad spectrum of industry except that the surveys of oil refineries
were disproportionately low in comparison to the volume of fluids handled.
This selection was deliberate because the petroleum industry handling
operations are more closely regulated than any other industry.  Three
integrated oil refineries and 21 oil terminals or storage areas were
surveyed.  Included in our survey were facilities of industries such as
Pharmaceuticals, paper, steel, food, beverages, detergents, paints, waste
processes, rubber, and textiles.  The results of these surveys are shown
in Table 20.
                                    69

-------
                                               TABLE 20
                 SUMMARY OF SPILL PREVENTION AND CONTROL PRACTICES AT 107 FACILITIES
                                                              Chemical Plants  (31)
This Study  (231
               Practices
Complete Dikec Storage
Tank Farm Level Alarms
Exclusive A'love Ground Transfer Lines
Curbed Process Areas
Process Area Catch Basins
Holding Lagoot.s
Primary Treatment
Secondary Treatment
Spill Cleanup Equipment
Preventative Maintenance Program
Spill Control Plan
LJL. A. * •*•
No.
47
8
12
23
14
18
33
6
17
19
42
Percent
44
8
11
22
13
17
31
6
16
18
39
No.
13
5
7
16
5
13
17
5
1
10
19
Percent
42
16
23
52
16
42
55
16
3
32
61
No.
12
2
8
11
6
10
12
2
3
8
14
Percent
52
9
35
48
26
43
52
9
13
35
60
                                             70

-------
     We note that in general, chemical plants have a higher utilization
of spill prevention and control practices than the average plant.  This
is probably caused by the greater number of hazardous materials handled
by these plants and the inherent potential hazard to personnel and
property.  In the present study, about one half of the facilities visited
were chemical plants.  Therefore in  the present survey, the utilization
of practices is closer to those reported for  chemical plants than for
the average of all plants,  of which  only 29%  were chemical plants.
                                      71

-------
                          VI.    ACKNOWLEDGMENTS
     The authors gratefully acknowledge  the asistance and cooperation of
many staff members of federal,  state  and local  regulatory agencies and
industrial facilities during  this  program.  We  are particularly indebted
to Mr. H. D. Van Cleave  of the  Division  of Oil  and Hazardous Materials,
Water Quality Office, of the  Environmental Protection Agency for his
support and guidance.  Mr. Howard  Lamp'l of the Edison Laboratories,
Mr. Anthony Resnick  of the California-Nevada  Basins  Region, Mr. Almo
Manzardo of the Great Lakes Regional  Office,  and Mr. John Latchford,
Clarence Johnson and William  Gross of the Texas Water Quality Board
assisted us in making arrangements for plant  visits.  The discussions
and comments with Mr. Joseph  Teller of the Texas Water Quality Board, and
Mr. Charles Bournes  of the Pacific Regional Office,  Environmental Pro-
tection Agency, also helped us  establish a meaningful field survey.
Finally we are most  appreciative of the  cooperation  and  assistance pro-
vided  to us by the more  than  50 operating facility personnel who devoted
much of their  time in frank and helpful  discussions  of water pollution
prevention methods with  us and  conducting us  on surveys  of their
facilities.  Cooperation such as this between industry and government
will ultimately be  the basis  for a valid pollution prevention program.
                                     73

-------
                            VII.   REFERENCES

[1]   Spill Prevention  Techniques  for Hazardous  Polluting  Substances,
      an Inventory  and  Survey of Hazardous Chemical  Facilities in
      Charleston, West  Virginia; Baltimore, Maryland;  Texas  City, Texas;
      and the  Suisan Bay-Delta area,  California; report  prepared by
      Arthur D.  Little,  Inc., under  Contract 14-12-927 for the Environ-
      mental Protection Agency, Water Quality Office,  Division of Oil
      and Hazardous Materials, February  1971.

[2]   The Prevention of Spills of  Oil and Chemicals  into Baltimore Harbor
      and Environs.  Report to Maryland  Environmental  Service, by Arthur
      D. Little,  Inc.,  May 1971.

[3]   Systems  Study of  Oil Spill Cleanup Procedures, Vol.  I, Analysis
      of Oil Spills and Control Materials, The Dillingham  Corp., Final
      Report to  American Petroleum Institute,  February 1970.

[4]   Proceedings of the Joint Conference on Prevention  and  Control of
      Oil Spills, American Petroleum Institute and the Federal Water
      Pollution  Control Administration,  December 1969.

[5]   Abstract of Proceedings of  the Hazardous Polluting Substances
      Symposium, sponsored by the  Department of  Transportation, United
      States Coast Guard, September 1970.

 [6]   Federal  Water Pollution Control Act as amended by  the  Federal Water
      Pollution  Control Act Amendments of 1961,  the  Water  Quality Act
      of  1965, the Clean Water Restoration Act of 1966 and the Water
      Quality  Improvement Act of  1970.

 [7]   Executive  Order 11507 - Prevention, Control and  Abatement of Air
      and Water  Pollution of Federal Facilities, February  4, 1970.

 [8]   Conservation Division, Branch of Oil and Gas Operations, Pacific
      Region,  United States Geological Survey,Outer  Continental Shelf
      Order No.  10, dated May 28,  1969.

 [9]   Conservation Division, Branch of Oil and Gas Operations, Gulf
      Coast Region, United States  Geological Survey, Outer Continental
      Shelf Order No. 1-10, dated  August 28, 1969 and  October 30, 1970.

[10]   Code  of  Federal Regulation,  Title 30, Mineral  Resources, Part 250,
      and Title  43, Public Lands,  Part 3380.

[11]   State of Rhode Island and Providence Plantations,  Oil  Pollution
      Control  Rules and Regulations, Rhode Island Department of Health,
      effective  September 1, 1957.

[12]   Division of Water Pollution  Control, "Rules for  the  Prevention and
      Control  of Oil Pollution in  the Waters of  the Commonwealth  ,
      Publication No. 5131, Commonwealth of Massachusetts-
                                      75

-------
                           REFERENCES Continued
[13]    Water  Pollution  Control,  Subchapter  4,  Prevention of Industrial
       Waste  Pollution,  Alaska Health and Welfare  Commission,  July 28,
       1959.
[14]    The Stream Control  Commission,  State  of  Louisiana,  "Rules
       Governing Disor.^1  or  waste  Oil,  Oil  Field Brine,  etc.",  as
       Amended January  27,  1953,  Title 56, Section 1435,  Chapter 3
       Part 1.

[15]    Railroad Commission of Texas, Texas Oil  and Gas  Conservation
       Laws,  Title 102,  January  1971.

[16]    Manufacturing Chemists Association, "Case  Histories of Accidents
       in the Chemical  Industry", Volume 1,  1962, Volume  2,  1966,
       Volume 3, 1970.

[17]    North Carolina Department  of Water and Air Resources,  Fifth
       Biennial Report,  July  1,  1966-June 30, 1968.

[18]    State of Rhode Island  and Providence  Plantations,  Department
       of Health, Environmental  Health Services,  Division of Water
       Supply and Pollution Control, Report  for the 12  Month Period,
       July 1, 1968-June 30,  1969.

[19]    Livingstone, F.  C.,"Combating the Menace of Oil  on Rivers",
       Water and Sewage Works, February 1971, p.  58.

[20]    "Hazard Survey of the  Chemical  and Allied Industries", Technical
       Survey No. 3, American Insurance Association,  1968.

[21]    National Fire Code,  Volume I, "Flammable Liquids",  National
       Fire Protection  Association, Boston,  Massachusetts 1969-1970.

[22]    Industrial Oily  Waste  Control,  prepared  by the American
       Petroleum Institute and American Society of Lubrication
       Engineers, 1969.

[23]    Crocker, B. B.,  "Preventing Hazardous Pollution  During Plant
       Catastrophes", Chemical Engineering,  May 4, 1970,  p.  97.

[24]    Spill Prevention Techniques for Hazardous Polluting Substances,
       and Inventory and Survey  of Hazardous Chemical Facilities in
       Charleston, West Virginia; Baltimore, Maryland;  Texas City,
       Texas; and the Suisan  Bay-Delta area, California;  report prepared
       by Arthur D. Little, Inc., under Contract 14-12-927 for the
       Kuviror .mental Protection  Agency, Water  Quality Office, Division
       DJ.' Oil ana Hazardous :.c.i.erials, February 1971.

[25]    The Prevention of Spills  of Oil and  Chemicals into Baltimore
       Harbor and Environs.  Report to Maryland Environmental Service,
       by Arthur D. Little, Inc., May  1971.
                                    76

-------
                          VIII.   APPENDICES


                                                                    Page

A.  Associations and Agencies Contacted by Letter  	    79

    Table 1:  Technical and Trade Associations
              Contacted by Letter	    80
    Table 2:  State and Municipal Agencies
              Contacted by Letter	    81

B.  Rhode Island Oil Pollution  Control Rules  and Regulations  .  .    85

C.  Selections from "Rules for  the Prevention and.  Control
    of Oil Pollution in the Waters of the Commonwealth of
    Massachusetts"  	    95

D.  Selected Regulations  of the Texas Railroad  Commission  ....   101

E.  Survey Guide	   107

F.  Detailed Results of Field Survey  	   113

G.  Typical Procedure  (Job  Standard) for Transfer
    Operation  in  Chemical Industry  - Typical Operating  Standard
    and  Check  List for Loading and  Discharging  of  Ships	   195
                                      77

-------
                 APPENDIX A




ASSOCIATIONS AND AGENCIES CONTACTED BY LETTER
                       79

-------
                               TABLE A-l

                    TECHNICAL AND TRADE ASSOCIATIONS

                           CONTACTED BY LETTER
                                                    REPLY       NO  REPLY
ASSOCIATION                                        RECEIVED     RECEIVED

AIME                                                                X
American Association of Oil Well Drilling
     Contractors                                                    X
American Foundrymens Society                                        X
American Iron and Steel Institute                                   X
American Paper Institute                                            X
American Petroleum Institute                          X
American Society of Civil Engineers                   X
Asphalt Institute                                     X
Chemical Specialties Manufacturing Association        X
Institute of Paper Chemistry                                        X
Lead Industries Association                           X
Manufacturing Chemists Association                    X
Metallurgical Society of AIME                                       X
National Agricultural Chemists Association            X
National Canners Association                                        X
National Paint, Varnish and Lacquer Association                     X
National Petroleum Refiners Association               X
Portland Cement Association                                         X
Rubber Manufacturers Association                                    X
Synthetic Organic Chemical Manufacturers Association  X
USA Standards Institute                                             X
Western Oil and Gas Association                                     X
Zinc Institute                                        X
                                   80

-------
                                               TABLE A-2
                                     STATE AND MUNICIPAL
                                          CONTACTED BY LETTER

                                                                         REPLY RECEIVED
ALABAMA
     Water Improvement Commission                                              No
     Bureau of Environmental  Health                                            No
ALASKA

     Department of Health  and Welfare                         Letter forwarded to Department  of  Environ-
                                                                   mental Conservation
     Department of Environmental Conservation                                  Yes
ARKANSAS
     Arkansas Pollution  Control Commission                                     Yes
     State Department  of Health                                                Yes
CALIFORNIA
     State Vater Resources Control Board                                       Yes
     Department of Public  Health                              Referred to Department of Conservation,
                                                                   Division of Oil and Gas
     Fire Marshall                                            Letter forwarded to State Water Resources
                                                                   Control Board
     Department of Conservation, Division of Oil  and Gas                       Yes
     State Wator Resources Control Board                                       Yes
COLORADO
     Colorado Department of Health                                             Yes
     Fire Marshall                                                             No

CONNECTICUT
     State Water Resources Commission                                          Yes
     State Department  of Health                                                No
     Fire Marshall                                                             No
DELAWARE
     Delaware Water  and  Air Resources  Commission                               Yes
     State Board of  Health                                                    No
     Department of Natural Resources and Environmental Control                 Yes
FLORIDA
     Department of  Air and Water Pollution                                     Yes
     State Board of Health                                                    Yes
     Department of  Natural Resources                                           Yes
     State Fire Marshall                                                      No
GEORGIA
     State Water Quality Control  Board                                         No
     Department of Public Health                                               Yes
ILLINOIS
     State Sanitary Water Board                                                Ko
     Department of Public Health                               Forwarded to Illinois Environmental Pro-
                                                                    tection Agency
     Environmental Protection Agency                                           Yes
     Chicago Fire Department                                                   Yes
     State Fire Marshall                                                       No
                                                    81

-------
                                     TABLE A-2 (Continued)
INDIANA
     Scream Pollution Control Board
     State Board of Health
     State Fire Marshall
KANSAS
     Kansas State Department of Health
     Water Pollution Control Section
     Fire Chief
     City-County Community Health Department
MARYLAND
                                                                          REPLY RECEIVED
                 No
                 Yes
                 Yes
                 No
                 No
                 No
                 No
     State Department of Water Resources                                       Yes
     Maryland State Department of Health and Mental Hygiene    Forwarded to Department of Water  Resources
MICHIGAN
     Water Resources Commission
     Department of Public Health
     Fire Marshall
MINNESOTA
     Minnesota Pollution Control Agency
     Division of Environmental Health
     Fire Marshall

 NEBRASKA
      Nebraska Water Pollution Control Council
      Department of Environmental Control
      Fire Marshall
 NEW JERSEY
      State Department  of Trl?:alth
      Department of Environmental Protection Agency
      Water Quality Branch,  Delaware River Basin
      Fire Marshall
 SEW MEXICO
      New Mexico Water  Quality Control Commission
 NEW YORK
      Fire Marshall - New York City
      Fire Marshall - Buffalo
      New York Department of Environmental Conservation
      Health Department
      New York State Petroleum Council
OHIO
     Water Pollution Control  Board
     Department of Health
     Fire Marshall
                 Yes
 Referred to Water Resources Commission
                 Yes
                 Yes
                 No
                 Yes
Referred to Department •;£ Environmental Control
                 Yes
                 Yea
                 No
                 Yes
                 Yes
                 Yes
                 No
                 No
                 Yes
                 Yes
                 No
                 Yes
                 No
                 Yes
                 Yes
                                                   82

-------
                                     TABLE A-2 (Continued)

                                                                         REPLY RECEIVED
OKLAHOMA
     Department of Health                                                     No
     Department of Pollution Control                                          Ho
RHODE ISLAM)
     Department of Health                                                     Yes
     Water Supply and Pollution Control                                       No
     Fire Marshall                                                            No
TENNESSEE
     Fire Marshall                                                            Yes
     Tennessee Stream Pollution Control Board                                 No
     Department of Public Health                                              No
VIRGINIA
     State Wattr Control Board                                                Yes
     Department of Health                                                     Yes
     Fire Marshall                                                            Yes
WASHINGTON
     Fire Marshall                                                            No
     Washington Water Pollution Control Commission                            Yes
     Department of Health                                                     So
 WEST VIRGINIA
      Fire Marshall                                                            Yes
      Department of Health                                                     So
      Department of Natural Resources                                          Yes
 WISCONSIN
      Department of Natural Resources                                          ^es
      Department of Health                                                     No


 NOTE:   other states—Pennsylvania, Maine, Massachusetts—were contacted by phone; written information
 was received.
                                                     83

-------
            APPENDIX B

RHODE ISLAND OIL POLLUTION CONTROL
      RULES AND REGULATIONS
                   85

-------
  fttatr of Ulfo&r inloub mt& Jlrantbrttre JHautnttnuu
OIL POLLUTION  CONTROL
RULES  AND  REGULATIONS
        Effective September 1, 1957
      Rhode Island Department of Health
       State Office Building, Providence, R. I.
                1957
                86

-------
              Rhode Island Department  of Health


  RULES   AND   REGULATIONS

                               OF THE

                      Department of  Health

  To Prevent the Discharge or  Escape of Any Petroleum,  Gasoline,
   Kerosene,  Tar, Asphalt,  Oil, or Any Product or Mixture Thereof,
            into the Waters of the State of Rhode Island

     1.  As used in these  rules and regulations  the word "person" shall
be held to mean and  include every individual, firm, co-partnership, asso-
ciation,  private corporation and municipal corporation, whether acting  as
principal, agent or servant, and whether acting personally or by agents or
servants, and  these rules and regulations shall apply  to each and every
such person.

     2.  As used  in these  rules and regulations the  term "oil" shall  be
held to mean  any petroleum, gasoline, kerosene, tar, asphalt, oil,  or any
product or mixture thereof.

     3.  As used  in  these rules  and regulations the  term "oil' carrying
vessel" shall be held to mean a vessel equipped to carry more than 5,000
gallons of bulk oil as cargo or as  fuel for her own use.

     4.  No person shall discharge, or  cause, suffer or procure to  be dis-
charged, or cause  or  suffer to escape, any  liquid waste, including storm
water runoff, or other waste,  into any of the waters of the state from any
new oil refinery,  new oil storage tank farm, new industry manufacturing
petroleum products, or new  industry  whose liquid waste or  storm water
runoff or other waste may contain oil, placed into  operation after these rules
and  regulations are established by order, unless plans and  specifications and
a description of a system or means to be installed to prevent the escape of
oil which may be present in such liquid  waste,  storm water runoff or other
waste have been submitted to the Department  of Health, and an order of
approval of the same has been entered by said  department.

     5.  No person shall discharge, or  cause, suffer or procure to  be dis-
charged, or cause  or  suffer to escape,  any oil into any  of the waters of
the  state; provided however  that this  rule shall  not apply to any waste
waters passed  through any oil separating or treatment equipment approved
by  the  Department of Health, and operated  in  a manner acceptable to
said department  and in  conformance  with any standards  of operation
contained  in said  department's order of  approval.

     6.  No person shall deposit, or  cause, suffer or procure to  be  de-
posited, any oil in any place on  the bank or  shore of any of the waters
                                 87

-------
of the state or  on any  wharf or pier  in  any such  waters, where the same
shall  be likely to be washed into  any of the waters of the state either by
heavy rains, high tides,  or storms, except hurricanes, or in any place where
the same shall  be likely to  be discharged or to  escape into any  of  said
waters.

     7.   No person shall  pump or  discharge, or  cause,  suffer or  procure
to be pumped or discharged  into  any harbor, river, bay, inland  waters or
any of the waters of the state, bilge or ballast water from any oil carrying
vessel  or from any other ship, barge, tanker, boat or vessel  whereby any
oil shall be liable to be discharged or  to  escape into any  of the waters
of the state.

     8.   No person shall scrape, wash, scrub, scour or swab, or cause, suffer
or procure to be scraped,  washed, scrubbed, scoured or swabbed, any  part
of any ship, barge, tanker, boat or vessel, or any  tank or  receptacle thereon,
while such ship, barge,  tanker, boat or vessel is  in any harbor, river,  bay,
or other waters of the state  or on any  shore thereof  or  in any  dry  dock
within the state, or any  oil tank or oil  receptacle  in  any place, whereby any
oil shall be liable to be discharged or to escape  into  any of the  waters of
the state.

     9.   No person shall transfer, or cause,  suffer or procure to  be trans-
ferred, any  bulk oil  from any oil carrying vessel  to  shore, or from shore
to any oil  carrying vessel,  or  ballast or cause, suffer  or procure to be
ballasted any oil carrying vessel unless the scuppers of any such vessel are
plugged  watertight during the oil  transfer or ballasting operation.

     10.   No person  shall  transfer, or  cause, suffer  or  procure  to  be trans-
ferred  any bulk oil  from any oil carrying vessel  to shore or  front shore to.
any oil carrying vessel unless  the  following precautionary measures  against
oil spillage into  the waters of the state during the transfer have been taken:

    a)   Any flexible hose  used  in the  transfer  which  has  not  been in
         regular use  shall have been tested at a pressure in excess  of  that
         to  which it will be subjected in use, and such test shall be made
         within one month previous to such use.

    b)  Drip pans are  placed under  hose connections on the oil carrying
         vessel, and drip pans  or a tight  wharf  or  pier section enclosed
         by a curb raised to  not less than four inches above  the  deck level
         is  provided under the  hose  connections on the  wharf or  pier. If
         drip pans are  used  they must  be in place before tight  blank, as
         provided in f)  of this rule, is removed and they must  remain in
         place until  blank is  replaced and hose is moved. This rule shall
         not prevent the instalation of e. drain to a tight curbed wharf or
         pier section  for the  removal of storm  water, provided  the drain
         is  tightly closed during any  oil transfer and no oil  contaminated
         drainage from  the  tight  section is  discharged into  the waters of
         the state, when the drain is open.
                                88

-------
    c)   I loses are  supported so  as  not to become crushed  between  the
         ship and the wharf or pier.

    d)   Hoses are  long  enough so that they will not be strained  by any
         movement  of  the ship  if the ship's mooring lines  are  adequately
         tended.
    e)   Mooring lines are tended frequently to prevent excessive move-
         ment of the ship at the wharf or pier.

    f)   Hose ends  are blanked tightly when hoses are moved into  position
         to be connected, and also immediately after they are  disconnected,
         before  they are  moved  away from their  connections.

     11.  No person shall transfer, or cause, suffer or procure to be trans-
ferred bulk oil from any oil carrying vessel to shore or from  shore to any
oil carrying vessel unless a man is stationed on the deck  of such vessel in
sight of  the hose and its vessel connections,  and  another man stationed on
shore in sight of the hose and its  shore  connections  continuously during
the transfer;  provided, however that in the case of the transfer^of oil to
or from  an oil barge, one man  stationed where  he can have  a clear view
of both the deck and the dock will suffice.

     12.   No person shall  transfer, or cause, suffer or procure to be trans-
ferred  bulk oil from any oil carrying vessel  to shore or from  shore to any
oil  carrying vessel  after  sunset and before sunrise  unless  decks  and  the
wharf or pier area  at the  point of transfer are brightly illuminated during
the transfer.

     13.   No person shall  transfer, or cause, suffer or procure to be trans-
ferred any bulk oil from  any oil carrying vessel to shore  unless:

     a)  All cargo  risers  not intended  for use in the transfer afe  blanked.

     b)  Sea valves connected to  the cargo  piping, and  stern loading con-
         nections are tightly closed and sealed with a numbered seal.

     c)   Lines and valves in  the  pumprooms and on deck  are checked by
         the ship's  master or senior deck officer to see that they are prop-
         erly set for discharging  cargo. An additional check is made for
         the same purpose each time  the setting  is changed.

     d)  Means of  communication  with shore  facilities  are  checked  and
         thoroughly understood.

     e)  Discharging is  started slowly until shore lines  are  proven  clear.

     f)   A check valve to prevent backflow  is located in  the discharge  line
         of  each oil cargo pump  of  a centrifugal type; the check  valve
         shall be located  at  a  point in the discharge line ahead of  any
         connection the  line makes with the discharge line  from any other
         cargo pump on the vessel.
     g)  A copy of the "Declaration of Inspection" required by the United
         States Coast  Guard  has  been handed to the terminal  superinten-
         dent or his representative, who shall  on  demand  be given  the
                                   89

-------
         opportunity to satisfy himself that the condition of the vessel  is
         as stated in the "Declaration of Inspection."

     14.  No person shall  transfer, or  cause, suffer or procure to be  trans-
ferred any bulk oil from shore to any oil carrying vessel  unless:

     a)   All sea valves connected to the cargo piping, stern discharge, and
         ballast discharge valves are  closed and sealed  with a numbered
         seal.

     b)   All hose  riser valves  not to be used are closed and  blank flanged,
         and all air valves on headers are closed.

     c)   Means of communication between  ship and  shore are  ascertained
         and all signals between ship and shore thoroughly understood.

     d)   Loading  is started  at a slow rate  and an inspection made of the
         ship's tanks to determine that all is going  according  to  plan before
         loading is increased to desired rate.

     e)   No more tanks are loaded at  one time than  can be safely watched
         and controlled.

     f)   Special attention is  paid  during  the  topping-off process  to the
         loading rate, the  number of tanks  open, the  danger  of  air pockets
         and the  inspection of tanks already loading.

     g)   To allow time for  orderly control, the slow down for  topping-off
         is anticipated and  notice  given to  shore personnel.

     h)   Water around the ship's side is  inspected  frequently, especially
         in the way  of the  seacocks, to  insure that  no oil  is escaping
         overboard.

     i)   Upon completion  of  loading, all  tank  valves and loading valves
         are closed. After draining, hoses are disconnected and  hose risers
         blanked.

     15.  No person shall ballast, or cause, suffer or procure to be ballasted
any  oil carrying vessel unless:

     a)   The transfer of cargo has been completed  and all hose  riser valves
         have been  closed and connections  blanked.

     b)   If ballast is to be pumped in,  whether  through deck lines or bottom
         line; valves on the lines used are  set first, then  the  valves to the
         tanks to  be  ballasted are opened,  the necessary  valves  in the
         pumprooms,  except seacocks, are  set  next,  and  cargo  pumps are
         started before opening seacocks.

     c)   If ballasting  is done  by gravity,  ballast is pumped in first for ten
         minutes  in accordance with  the procedure  outlined  above  in b)
         to clear all bottom lines of oil.

     d)   When ballasting is started, all tanks are inspected to see that only
         toe tanks intended are receiving ballast.
                                    90

-------
    e)   The  same attention  is given to ballasting as to topping-off tanks
         when loading cargo.

    f)   When completing the loading of ballast, seacocks are closed before
         stopping the pumps.

    The provisions of  a), b), c),  f)  of  this rule shall not apply  to  any
vessel whose ballast  piping system  and ballast pumps are wholly indepen-
dent and not  connected  to the cargo system,

     16.   No  person shall discharge, suffer  or  procure to be  discharged,
the exhaust  steam  from any coil  or  other  device  used to heat oil,  into
the water of  the state  or into any public sewer or storm  drain, or  into
any private drain which empties into any  of the waters of the state or onto
the banks of  any of these waters unless such exhaust steam is  first passed
through  an oil removal  system approved by the Department  of Health.

     17.   No  person shall discharge  the  drainage from any Underground
pipe gallery used as  a conduit for oil pipes, or the drainage frpm the floor
of any boiler room where oil burning equipment is located, into a public
sewer or storm drain or  into the  waters of the  state or onto the banks of
these waters  without first passing the  drainage through an  oil  removal
sysem approved  by the Department of Health.  This rule shall  apply only
to the drainage  from business and industrial establishments.

     13.   No  person maintaining a dike  around an oil storage  tank  shall
have  any openings in  such dike that will permit the escape of drainage
from behind  the dike  into any sewer or drain or into the waters of the
state.

     An  opening such as a pipe provides, may be placed in the dike provided
it is kept closed at all times except for periods, no longer than are necessary,
to  remove accumulated  drainage.  When it is  necessary  to remove  such
drainage it shall be passed thru an  oil removal  system approved  by the
Department of Health, unless it is  wholly oil free. If free of oil it may be
discharged as desired. If  temporary openings in the dike  are made to permit
doing work on or inside  the same,  provision must be made while the open-
ings exist to  convey 4rainage from the dike to an oil  removal  system ap-
proved  by the  Department of Health, or other provision made  to prevent
such  drainage from  reaching the waters  of the state without the removal
of any oil it  may contain.

     19.   Every person operating a terminal for the transfer of oil  from
ship to shore or from shore to ship shall, when  a spillage of oil occurs at
his terminal,  take steps immediately to contain  the spilled oil, and  remove
it from  the  water if any has reached  it. For this purpose he  shall  have
readily available adequate essential  equipment approved  by the Department
of Health and personnel familiar  with such salvage operations.

     20.   Every person operating a terminal for the transfer of oil  from
ship to shore or from shore to ship shall inspect every ship using his ter-
                                 91

-------
minal and  fill out the inspection report supplied to him by the Department
of Health, and submit  the  same  to  said  department  promptly  when  the
ship has led the terminal.

     21.  Every person who  handles oil shall, when a spillage of  oil occurs
on his premises,  take steps as  promptly as possible  to prevent the spilled
oil from reaching a public sewer or drain or  in any way any of the waters
of the state.

     22.  No  person  shall discharge the  drainage from any bulk oil plant
yard, refinery area, or other  outdoor area where large volumes of  oil (more
than  21,000   gallons) are received or  stored  or shipped, and where by
accident or otherwise oil may escape or be spilled into  any public sewer or
drain or into any of the waters of  the state,  without first passing such
drainage through  an oil  removal system approved by the Department of
Health. This  rule shall not prevent  the discharge into any  publfc sewer
or drain or into the waters of  the  state of  any oil  free drainage from such
areas if means are provided  to retain the drainage for inspection  befort it
is discharged  and only oil free  drainage  is  so discharged.

     23.  No  person  shall maintain a vent to any  oil storage tank located
on the premises of a business or industrial establishment that is filled through
an  opening in the top of the  tank except one carried at least three  feet
higher than the opening, in order that the oil will first overflow at the inlet
to the tank if the tank  is filled beyond its capacity.  This rule  shall  not
apply to a tank  used to store  only fuel oil of a grade which  will -flow at
all times without being heated.

     24.  No  person  shall maintain an inlet  to an  oil storage tank located
on  the  premises of a  business  or  industrial  establishment except one so
located or  protected  that  should the  tank  overflow accidentally on filling,
the oil will be retained near the tank and  will not reach  any public sewer
or drain or the waters of the  state.  This  rule  shall not  apply to a tank
used  to store only fuel oil which will flow at all times without being heated.

     25.  No  person  shall permit any oil pipe to  leak oil in any  location
where the oil  may be washed or drained into a storm drain or sewer or into
the waters of the state.

     26.  Every  person shall post  and keep posted such  'warning signs or
copies of extracts of these rules and regulations as  may be provided  to him
by the Department of Health,  in a conspicuous place where the same may
be  easily  read, at each of the wharves  and piers  owned, leased,  operated
or controlled  by such person,  and  at each separate  parcel of  land owned
or leased by such person which borders on, or any part of which is within
one hundred feet of any of the waters within the state, and whereon there
is deposited or stored at  any  one  time, any oil, in  greater quantity  than
twenty-one thousand  gallons.
                                   92

-------
     27.  These rules and reputations shall be  in  full  force and effect on
and  afler the first day  of September A.D.  1957 and any previously  issued
orders establishing rules  and regulations  to  prevent  the  discharge  of oil
into the waters of the  state are hereby declared to be null  and void, on
and  after that date.

     Ordered on the twelfth day of  August A.D. 1957.

     Violations of  an order of the Department of Health are punishable by
a fine of not more than five hundred dollars ($500.00) or  by imprisonment
for  not more than one (1) year, or by both  such fine and imprisonment.
(Section 14, Chapter 12, Title 46, General Laws of 1956).
                                 93

-------
                            APPENDIX C

       SELECTIONS FROM  "RULES FOR THE PREVENTION AND CONTROL
OF OIL POLLUTION IN THE WATERS  OF THE COMMONWEALTH OF MASSACHUSETTS"
                                  95

-------
Section /«.n--MAR!NF. Oil. TERMINAL TRANSFER OPERATIONS

      Particular care is essential to prevent oil pollution cause by
spills during transfer of bulk oil from a vessel to shore, or from
shore to a vessel or during ballasting.
Section 4.01--PRE-TRANSFER CONFERENCE

      Prior to commencing oil transfer operations, the following items
shall be understood and agreed by both vessel and shore personnel in
responsible charge of operations:

      a.  Cargo sequence for loading or discharging products.

      b.  Handling rate at which oil will be transferred.  Reduced
          rates are required when commencing ransfer, changing the
          lineup, topping off tanks, or nearing completion of transfer.
          The amount of standby time to be given when the vessel or
          terminal desires to start, stop, or change the rate of flow
          must be agreed upon.
      c.  Adequatp communication and signal systems must be established
          and checked, and must be readily available during transfer
          operations.

      d.  Emergency procedures to be followed in order to stop and con-
          tain any spillage must be understood.
Section A.02—VESSEL OPERATIONS

      During oil transfer operations, the following procedures shall be
followed by vessel personnel:

      a.  A licensed officer or certified tanker-man who has full know-
          ledge of the vessel's tanks and cargo handling system shall
          be in charge of cargo handling.

      b.  A sufficient number of adequately-trained men shall be on duty
          during cargo operations.

      c.  The vessel shall be moored with adequate lines to prevent sur-
          ging, and the mooring lines shall be properly tended to pre-
          vent the lines from either parting or developing excess slack.
      d.  All scuppers shall be plugged during transfer operations.  If
          scuppers must be unplugged to drain water from the deck area,
          they shall be tended constantly and the plugs replaced immediately.
          No oil or emulsion shall be discharged through scuppers.

      e.  The ends of hoses or other connecting devices shall be blanked
          while being put in place.  A drip-pan shall be used at the cargo
          or bunker manifold when removing the blank and making up the
          connection.  The drip-pan shall be left in place during transfer
          operations.  Connections shall be secured to insure against
          leakage.  Flanges, joints and hoses shall be checked visually for
          cracks, weak spots or points of excessive stress.
                                  96

-------
     f.  Before commencing transfer operations,  the initial  lineup
         shall be  checked  from the deck manifold connection  through
         the  system to the first tank valve to see that rilTOs  are
         properly  set.  All valves which are not involved in initial
         transfer  operations must be closed tightly.  Sea-valves  con-
         nected  to cargo or bunker piping systems, stern discharge
         and  ballast discharge valves shall be closed and sealed
         during  transfer operation.

     g.  During  transfer operations, a man or men shall be stationed
         where vessel connections, hose and terminal connections  can
         be observed.  Regular inspections shall be made of  the trans-
         fer  lineup,of water around the vessel,  and of connections
         and  other points subject to leakage.

     h.  On completion of transfer operations, hoses or other connect-
         ing  devices shall be vented, blown down, or sucked  out to
         drain  the remaining oil.  A drip-pan shall be used  when
         breaking a connection, and the end of the hose or other  con-
         necting devices shall be blanked off before being moved.

      i.  During  ballasting, pumps shall be started before opening
         sea-valves, and pumps shall be stopped after closing sea-valves.
Section A.03—TERMINAL OPERATIONS

      a.  Procedures outlined in Section 4.02 for vessel operations  also
          apply to terminal operations where appropriate.

      b.  A tight wharf or pier section enclosed by a curb is satisfactory
          in place of drip-pans, provided no oil-contaminated drainage is
          discharged into the waters of the Commonwealth.

      c.  Before commencing discharge of dirty ballast or slop-oil to
          terminal facilities,  the system and lineup shall be checked.
          During transfer the system shall be checked regularly for
          leakage.

      d.  Where waste oil collection and separation facilities are in-
          stalled, the separator shall be checked regularly for proper
          operation.

      e.  Care shall be taken to prevent leakage or 'spillage of oil from
          drip-pans when they are dumped for disposal.

      f.  Terminal operators shall have a maintenance inspection and test-
          ing program for all oil-handling hoses and equipment in order
          to detect faulty equipment.
                                  97

-------
Section 4.04--USE AND CARE OF HOSE

      a.  Any hose used in oil transfer service shall be of a grade
          suitable for oil service and be designed to withstand pressure
          of the shut-off head of the pump or pump relief valve setting.
          Such hose shall be tested annually at a pressure In excess of
          that to which It Is subjected In use.

      b.  Hoses shall be supported during transfer operations so as not
          to be crushed between the vessel and wharf or to be subjected
          to strain due to excessive curvature.

      c.  Hose lines shall be sufficiently long and adequately supported
          so as not to be strained excessively by any movement of the
          ship due to tides or change in draft during oil transfer
          operations.

      d.  Hoses shall not be permitted to chafe on the dock or ship, or
          to be in contact with hot surfaces such as steam pipes, or to
          be exposed to other corrosive sources*
                                 98

-------
Section 5.0—TERMINALS. BULK PLANTS & OTHER  INSTALLATIONS HANDLING OIL

5.01  All terminals and bulk plants shall  be so  located  and constructed
      as to provide against flooding by high water  and  the accidental
      discharge of oil to water  courses.

5.02  Proper maintenance measures  shall be provided and  due caution
      exercised to prevent any spills or discharges of oil to water
      courses.

5.03  Any drainage which may contain oil in  such amounts as to cause, or
      contribute  to,  a condition in contravention of the established water
      quality  standards must first be passed through a properly maintained
      and adequate oil-trap or other oil removal system  approved by the
      Division.                                         '

      This  shall  include,  but  not be  limited to:

      a.  Surface drainage from any oil-contaminated area of a terminal,
          bulk oil plant  yard  or other  outdoor area where large volumes
          of bulk oil are received or  stored, or shipped.

      b.  Drainage  from  any pipe trench or pipe gallery  used as a conduit
          for  oil pipes.

      c.  Exhaust steam,  condensate or  water from any device used to heat
          or cool oil.

 5.04  Each  permanent oil storage tank or battery of tanks must be sur-
       rounded  by a  dike  or retaining  wall of sufficient capacity  to con-
       tain  spillage  and  prevent pollution of the surrounding areas.  Ac-
       cumulated drainage shall be removed through a properly maintained
       and adequate  oil-trap or other  oil removal system approved  by the
       Division.
                                    99

-------
                      APPENDIX D




SELECTED REGULATIONS OF THE TEXAS RAILROAD COMMISSION
                          101

-------
RULE 8.  WATEft gROTECTlOK

    (A)  Fresh Watet to be Protected

          Freeh water, whether above or below the surface, shall

be protected from pollution whether lit drilling, plugging, pro-

ducing, or disposing *£ salt water already produced.

    (B)  Exploratory Wftlla

          Any oil or gas well or w«ll drilled for exploratory pur-

poses shall be governed by the provisions of statewide or field

rules which are applicable and pertain to the drilling, safety,

casing, production, abandoning and plugging of wells, and all
                                            >
operations in connection therewith shall be carried on so that

no pollution of any stream or water course of this State, or any

subsurface waters, will occur as the result of the escape or re-

lease or injection of oil, gas, salt   water or other mineralised

waters from any well.
                                  102

-------
(As added by Order No. 20-56,8Hl, effective  1-1-69).
     (C) (1)  All operators conducting  oil and gas. development and
production operations are prohibited  from using  salt water disposal pits
for storage and evaporation of  oil  field  brines  and mineralized waters.
         (a)  The provisions of this  rule do not affect the use of
burning pits which are used exclusively for  the  burning of tank bottom
waste accumulation.
         (b)  Impervious  collecting pits  may be  approved  for use in
conjunction with approved salt  water  disposal operations, provided that
authority must be received for  use  of such pits  from the  Commission.
         (c)  Discharge  of oil  field  brines  and  mineralized waters into
a  surface drainage water course, whether  it  be a dry creek, a flowing
creek or a river, except where  permitted  by  the  Commission, is not an
acceptable disposal  operation and is  prohibited.
          (d)  Disposition of oil field brines and mineralized waters
through off-lease facilities where  transportation is by tank trucks, pipe-
 lines or other means,  is the  initial  responsibility of the lease operator
and shall not be initiated until such method of  disposition is permitted
by the  Railroad Commission.   Such permit  shall be subject to review and
cancellation should  investigation show that  the  permitted method of
disposition  is abused.
         (2)  Exceptions  to the  provisions of this rule may be granted
by the  Railroad Commission on  special request where good  and sufficient
cause is shown.
         (3)  Penalty for non-compliance with any part  of  this rule
shall be pipeline severance for each  lease  operated in violation of this
rule.

                                           103

-------
       (U)  In any instance where a salt water disposal pit is



presently in use and is abandoned, due to cessation of flow of salt



water thereto, whether voluntary or mandatory, such pit shall be back-




filled and compacted.



     (D)  Pollution Prevention



     (As added by Order No. 20-59,200, effective 5-1-69)



     (1)  The operator shall not pollute the waters of the Texas



offshore and adjacent estuarine zones (salt water bearing bays,



inlets, and estuaries) or damage the aquatic life therein.



     (2)  All oil and gas well drilling and producing operations



shall be conducted in such a manner to preclude the pollution of the



waters of the Texas offshore and adjacent estuarine zones.  Particular-



ly, the following procedures shall be utilized to prevent pollution.



          (a)  The disposal of liquid waste material into the Texas



offshore and adjacent estuarine zones shall be limited to salt water



and other materials which have been treated, when necessary, for the



removal of constituents which may be harmful to aquatic life or



injurious to life or property.



          (b)  No oil or other hydrocarbons in any form or combination



with other materials or constituent shall be disposed of into the



Texas offshore and adjacent estuarine zones.



          (c)  All deck areas on drilling platforms, barges, work-



over unit and associated equipment both floating and stationary subject



to contamination shall be either curbed and connected by drain to a



collecting tank, sump or enclosed drilling slot in which the contain-



ment will be treated and disposed of without causing hazard or pollution;



or else drip pans, or their equivalent, shall be placed under any equip-




                                     104

-------
ment which might reasonably be  considered a source  from which
                                                  -?:>
pollutants may escape  into surrounding water.   These drip pans must

bc« piped to collecting tanks,  sumps or enclosed drilling slots

designed to accommodate all reasonably expected drainage.   Satisfac-

tory means must be  provided to empty the sumps or enclosed drilling

slots to prevent overflow or prevent pollution of the surrounding water.

           (d)  Solid combustible waste may be burned and the ashes

may be  disposed  of  into Texas offshore and adjacent estuarine zones.

           Solid wastes such as cans, bottles, or any form of trash

must be transported to shore in appropriate containers.  Edible garbage,

which may  be  consumed by aquatic life without harm, may be disposed of

 into Texas offshore and adjacent estuarine zones.

           (e)  Drilling muds which contain oil shall be transported

 to shore or a designated area for disposal.  Only oil-free cuttings

 and fluids from mud systems may be disposed of into Texas offshore

 and adjacent estuarine zones at or near the surface.

           (f)  Fluids produced from offshore wells  shall be mechan-

 ically contained in adequately pressure-controlled  piping or vessels

 from producing well to disposition point.  Oil and  water separation

 facilities at offshore and onshore locations shall  contain safeguards

 to prevent emission of pollutants to the Texas offshore and adjacent

 estuarine zones prior to proper treatment.

           (g)  All deck areas on producing platforms subject to con-

 tamination shall be either curbed and connected by drain to a. collect-

 ing tank or sump in which the containment will be treated and disposed

 of without causing  hazard or pollution, or else drip pans, or their

equivalent,  shall be placed under any equipment which might reasonably


                                       105

-------
be considered a source from which pollutants may escape into surround-



ing water.  These drip pans must be piped to collecting tanks or sumps



designed to accommodate all reasonably expected drainage.  Satisfactory



means must be provided to empty the sumps to prevent overflow.



          (h)  Any person observing water pollution shall report such



sighting, noting size, material, location and current conditions to



the ranking operating personnel.  Immediate action or notification shall



be made to eliminate further pollution.  The operator shall then trans-



mit the report to the appropriate Commission district office.



          (i)  Immediate corrective action shall be taken in all cases



where pollution has occurred.  An operator responsible for the pollution,



shall remove immediately such oil, oil field waste, or other pollution



materials from the waters and the shore line where it is found.  Such



removal operations will be at the expense of the responsible operator.



     (3)  The Commission may suspend producing and/or drilling opera-



tions from any facility when it appears that the provisions of this



rule are being violated.



     (U) (As added by Order No. 20-60,2lU, effective 10-1-70)



         The foregoing provisions of Rule 8(D) shall also be required



and enforced as to all oil and gas operations conducted on the inland



and fresh waters of the State of Texas, such as lakes, rivers, and



streams.
                                    106

-------
 APPENDIX E




SURVEY GUIDE
       107

-------
                              SURVEY GUIDE






A.  STORAGE. TRANSFER. LOADING AND UNLOADING



        These facilities are intended to include tank farms for raw and



refined products from which transfers are made for transportation to



non-contiguous areas for use or further processing.  In the case of petro-



leum products or certain other hazardous, combustible products, a number



of legal requirements exist as to the location of tanks within diked areas



of definad configurations.  However, many tank farms for hazardous pollut-


ing substances do not now have such protection against movement of spilled



liquids and the interviewer should consider questions of the following

                                                 s

type:



        (a)  What are typical fail-safe procedures and equipment employed



            for filling and emptying storage tanks, e.g., are the pumps



            equipped for automatic shutdown on high-level indication in



            a tank being filled; are lines entering the tanks located so
                              •i

            that siphoning effects are prevented in the case of line



            breakage; in the case of long lines of large diameter, what



            provisions are made for liquids draining out in case of


            rupture, etc.?



        (b)  In diked storage tank areas, how is rainfall runoff handled,



            i.e., is there an installed drainage system which is pro-



            vided with normally shut valves; is ground seepage adequate



            to remove rainfall—if so, what about  ground water pollution?



            Does the rainfall go to a holding basin or through a waste-



            water treatment plant before it can enter water courses?




                                   108

-------
(c)   Are tanks equipped with remote level sensing and alarming




     systems sounding into a central location?




(d)   What administrative procedures are in effect concerning



     notification of spills?




(e)   Are there any unique regulations based on experience or




     safety requirements that dictate certain design procedures,




     for example, the generation of electrostatic charges by




     discharging the entering liquid above the surface of the




     liquid in the tank?




(f)  What design standards are  presently used for the trans-




     portation equipment of concern, i.e., are these standards




     developed by an industry group, promulgated by insurance




     companies, defined by the  carriers, or established by the




     equipment owners?




(g)  Are operators of  transportation equipment familiar with




     the type of cargo, methods for controlling and combating




     spills, and/or know how  and where  to  seek rapid assistance




     in the case of an  accidental spill?   For example, is the




     MCA's Chem-Card Manual utilized?




(h)  Since an accidental spill  of a hazardous polluting substance




     is most often best combated by containment in a localized




     area followed by  removal  for disposal, what types of equip-




     ment are carried  for  effecting such an operation?  For




     example, a tank  truck operator might  be expected to have




     available shovels  for creating small  dikes to prevent rapid




     migration into water  courses.



(i)  What fire, explosion  and personnel safety requirements  are




     now demanded by  regulatory groups  and how do  these





                             109

-------
            requirements  affect  the prevention or detection of spills


            and leaks?



B.  PROCESSING PLANTS


        Questions should  be based on the fail-safe concepts of operation


and hardware that are presently  installed to meet (1)  personnel safety


regulations, (2) preventing loss of valuable materials, (3) fire insur-


ance or other codes, and  (4) protection of equipment.   Interviewers


should be especially alert to in-plant procedures for  coping with spills


especially to such operations as water flushing for safety or removal


reasons and what procedures are  utilized to prevent spilled hazardous


polluting substances (HPS) from  entering surface and ground waters.


       (a)  What fail-safe procedures are incorporated in the process


            designs and operational procedures?  For example, are pres-


            sure, temperature, liquid level, and flow  rate sensors


            alarmed?  Do these sensors actuate the closing of valves,


            the shutdown of pumps, or a fire protection system?  Are


            there any special fail-safe procedures required, for insur-


            ance regulations or  by legal or other codes?

                                                           j)
       (b)  Are process areas curbed on a selective basis, i.e., with


            respect to the volume and specific degree  of hazard


            involved in the material handled?


       (c)  How is the drainage from the plant and the process areas


            handled?  For example, are there separate sewer systems


            from process pads going to special waste-water treatment


            facilities?  If curbed areas are unable to contain the


            maximum credible spill, i.e., the maximum volume present


            in the processing units located in the area, where would



                                    110

-------
     the overflow go, i.e., into storm sewers draining directly




     to water courses, to holding basins, to municipal sewers,



     and so on?




(d)   Where holding basins  (used for surge capacity) are in-




     stalled so that runoff or overflows can be treated prior




     to discharge to water courses, what is the design basis?




     For example, the maximum 24, 48, etc., hour rainfall over




     a 10, 20, 50 year or  other period?




(e)   Before a holding or catchment basin is emptied, what de-




     cisions are made as to whether the contents are emptied




     through treatment plants, or directly into receiving




     waters?  What analytical procedures are carried out?




(f)  Are special handling  equipment, or treating agents, e.g.,




     lime  for acid neutralization, located throughout the




     plant for cleanup of  spilled substances?




(g)  Is there any special, non-process, detection instrumenta-




     tion  now installed  that has a sole function of alarming




     if spills occur?  What type of detection equipment is




     now installed for safety reasons and what is the nature




     of any process  controls actuated by this equipment?




(h)  What  degree of  reliability  is placed upon present de-




     tection and alarm sensors,  especially with respect to




     experience and  the  backup or spare philosophies incor-




     porated in design and operation.




(i)  What  has been the major attributable  causes for past




     in-plant spills regardless  of size or whether  these
                             111

-------
entered receiving waters,  for example, process equipment




failure, operator error, control equipment failure and




so on.
                      112

-------
           APPENDIX F




DETAILED RESULTS OF FIELD SURVEY
                113

-------
         DESIGN CRITERIA, EQUIPMENT. AND PROCEDURES IN CHEMICAL FACILITY - PLANT^A
                      ITEM

1.  Drainage ditches surrounding acid tanks
    lead to neutralization area

2.  Spare acid tanks for rapid transfer in case
    of leaks in primary tanks

3.  Scheduled manual gauging of all storage tanks
    once per shift

4.  Tanks dikad to prevent spills from entering
    waterway
                                                      TYPE

                                                      Design criteria,
                                                      equipment

                                                      Equipment
                                                      Procedure
                                                      Design criteria,
                                                      equipment
AREA_

Storage


Storage


Storage


Storage
5.  Reduce number of flanges in piping systems
    to reduce leaks

6.  Pipelines located overhead (above grade) to
    help locate leaks

7.  Metal articulated swivel joint loading arms
    for liquid transfer to rail and tank cars

8.  Concrete gutters (curbing) along rail and
    truck unloading areas to convey spills to
    neutralization or treatment area

9.  Gravel covered loading and unloading points
    to prevent runoff

10. Concrete surfaced pad surrounded by curbing
    and/or drainage ditch in process area

11. Large centrally located lime slurry tank for
    neutralization

12. Common neutralization facility in addition
    to principal waste treatment facility

13. Continuous pH monitoring to detect spills
    or leaks in main waste treatment stream

14. Discharge to county waste treatment
    facility on a fee basis
                                                      Design criteria


                                                      Design criteria


                                                      Equipment
                                                      Equipment,
                                                      design criteria
                                                      Design criteria


                                                      Design criteria,
                                                      equipment

                                                      Equipment


                                                      Equipment
                                                      Equipment and
                                                      procedures
Transfer
Transfer
Loading and
unloading

Loading and unload
ing, waste treat-
ment

Loading and
unloading

Process
Process, loading
and unloading

Waste disposal


Waste disposal


Waste disposal
Principal Hazardous Materials

Inorganic acids;  chlorinated rubbers  and waxes,  ammonia,  chlorine,  alcohols,  toluene, wax,


                                             .114
chlorinated hydrocarbons

-------
                               PLANT A  (Continued)
REQUIRED OR USED BACK-UP  SYSTEMS

Neutralization area required
REMARKS
                                         For acid  tanks only
Sight  tubes and float  gauges  used
also

Fail-safe system for dike
valves required
Continuous inspection required to
identify leaks
Acid tanks diked; alcohol
tanks diked to prevent loss
of costly fluid

Efforts made in all new lines  to weld
joints because of leaky flanges
                                         Experience  indicates loading arms are
                                         more  reliable than flexible hoses
Adequate neutralization area required  Mostly used for acid areas and spills
                                        May actually be detrimental since acids can
                                        enter  ground water; curbing may be better
Adequate neutralization or holding
area required

Distribution method  for slurry and
disposal of material required
Neutralization  facility and
equipment required
                                         Prevents overloading of waste treatment
                                         facility in case of spills
                                         This  is a  back-up system for waste treatment
                                         facilities;  is used when overloaded
                                          115

-------
          DKSICN CRITERIA,  EQUIPMENT,  AND PROCEDURES-IN CHEMICAL FACILITY  - PLAHT__B
                      IT KM

i.   Storage tanks  of  hazardous materials  are
    diked

2.   Tanks  containing  hazardous materials  have  no
    bottom connections;  fluids pumped from top

3.   Storage tanks  have high level alarms  and
    "high-high" levels shutoff for pumps

4.   Overflow lines from tanks run to process
    area ditch

5.   Major  valves may  be locked to prevent
    unauthorized use               i

6.   Special toxic  materials stored in underground
    concrete tanks with impervious membrane layer
    in tank walls

7.   Flange bonnets used on mechanical pipe
    connect ions

8.   Closed sections of lines protected with relief
    valves and burst disks

9.   Written procedures for all operations from
    transfer to processing; sign-off sheets
    checked step by step by operator, filed
    for record

10. Materials are sampled and analyzed for
    compatability before transfer operations

11. Manual (stick level) gauging done periodically
    to check instrumentation

12. Written permission of supervisor required to
    override safety shut-off system

13. Different type (design) couplings for
    different substances

14. Transfer areas sloped and graded toward
    process drains

15. Rail  transfer areas curbed, with sump for
    spills; liquid must be pumped from sump

16. Process areas sloped toward process area
    ditches and drains

17. Rainwater ditches separate from process drain;
    used  to drain swampy areas direct to  river
T)TK

Design criteria,
equipment

Design criteria,
equipment

Equipment
Equipment
Procedure
Design criteria,
equipment
Kquipment
^quipment
Procedure
Procedure
Procedure
 Procedure
Design  criteria,
equipment

Design  criteria
 Design criteria,
 equipment

 Design criteria
 Design criteria
ARFA

Storago


Storage, process


Storage, process


Storage, process


Storage, process


Process, storage



Transfer


Transfer
Storage, transfer
process
Storage,  transfer


Storage,  transfer


Storage,  transfer
process

Transfer,  loading
and  unloading

Transfer,  loading
and  unloading

Loading  and
unloading

Process


Process,  other
                                              116

-------
REQUIRED OR USED BACK-OP  SYSTEMS
                                         PLANT B (Continued)
                                                REMARKS
Alarms and indicators  are located in central
control room, manned continuously
 System for collection or drainage of
 any vented materials required
                                                There are no penetrations in dikes;  fluids
                                                are pumped out if contained in diked area

                                                Prevents leakage from valves by gravity
                                                flow
                                                This is a back-up system to convey overflows
                                                to holding areas.

                                                Has both advantages and disadvantages as a
                                                fail-safe system

                                                Prevents toxic material from entering ground
                                                water
                                                Prevents leaks in and damage to flange
                                                joints
                                                Supplements fail-safe equipment and design
                                                criteria; helps operator reduce possibility
                                                of accidents
                                                Prevents chemical reactions—primarily a safety
                                                procedure which can act as a pollution control measure

                                                Check on fail-safe instrumentation
                                                 Prevents  accidental flows of materials to
                                                 wrong  lines  or  tanks—mainly a safety feature
 Adequate process waste treatment  required
 Sumps must be large enough  to  handle
 maximum spill

 Process drain system required
Used only for most hazardous or toxic materials
 Method to ensure that  spills  cannot get into
 rainwater ditches required
                                                  117

-------
 DESIGN CRITERIA,  EQUIPMENT, AND PROCEDURES IN CHEMICAL  FACILITY -  PLANT B /Contj.nued)
                      ITEM

18.  Process areas hard surfaced

19.  Fire control deluge water flows into process
    area ditch

20.  Separate holding basins in each process area
21. Holding basin with 24-hour capacity

22. Double capacity emergency basin


23. pH monitors at inlets to each basin
24. pH instruments checked three times daily by
    grab samples and lab analysis

25. Visual checks periodically for oil downstream
    of skimmers

26. Heavy metal and other pollutants monitored

27. Settling basins have membrane liner to
    prevent seepage

28. Well points surround settling basins sampled
    to check for leakage
TYPE

Design criteria

Design criteria
Equipment, design
criteria

Equipment

Equipment, design
criteria

Equipment
Procedure


Procedure


Procedure

Equipment


Procedure
AREA

Process

Process


Process


Waste treatment

Waste treatment
Process, waste
treatment

Waste treatment
Waste treatment


Waste treatment

Waste treatment


Waste treatment
Principal Hazardous Materials

Chlorinated hydrocarbons, inorganic acids, caustic, oil, metal alkyls, acetone, kerosene
                                        118

-------
                                          PLANT B (Continued)
REQUIRED OR USED BACK-UP  SYSTEMS
Fire control deluge water may contain
hazardous materials and requires treatment
REMARKS

Some process storage tanks with volatiles on gravel
                                               Each process area has holding basin of capacity
                                               equal  to all tanks and equipment in area

                                               This is a back-up for holding tanks in process areas

                                               This is a back-up for large spills; fluids must
                                               be diverted to basin

                                               Used to activate caustic addition system to
                                               neutralize waste streams

                                               This is a back-up measure to ensure automated
                                               equipment works well

                                               Check  on equipment     -
                                                Used to check if spill  has  occurred or as process control
                                                Back-up system to detect faulty operation
                                                   119

-------
DESIGN CRITERIA. PROCEDURES AND EQUIPMENT IN OIL STORAGE AND TERMINAL PACILITY*_r_ PLANT C
                      ITEM

1.  All storage tanks for oil and  hydrocarbons
    are diked

2.  Process sewer system for drainage of  fluids
    in diked areas
TYPE

Design criteria,
equipment

Equipment
3.  Leak detection system for pipelines—consisting    Equipment
    of flow meters and meter provers,  with computer
    system to check input and output

4.  Separate sumps provided at blending,  packaging,    Design  criteria,
    and loading facilities                            equipment

5.  Standard procedures for draining flexible hoses    Procedure
    after loading by gravity for barge operations
6.  Standard procedures for pumping to drain
    flexible hose lines on tanker operations

7.  Temporary mounted high level alarms in barges
    to provide visual and audio alarm on filling

8.  All process units on hard surface pads

9-  Standard procedure for flushing and draining
    sample lines into process waste sewer

10. Once through cooling water visually inspected
    and instrumented for measurement of total
    organic carbon before discharge back to river

11. Waste water effluent from solvent recovery
    and other process units monitored for
    dissolved carbon

12. Impending area for rainwater to handle
    24-hour drainage from worst storm in seven-
    year period

13. Most of area served by two waste systems,
    one for only water, the other clean

14. Chemical waste water kept separate from oily
    waste water

15. Turbidity monitor for water leaving oil/water
    separator
Procedure


Equipment


Design criteria

Procedure
Procedure,
equipment
Procedure,
equipment
 Equipment



 Equipment,
 design  criteria

 Design  criteria


 Equipment
AREA

Storage, process


Storage


Transfer
Loading and
unloading

Loading and
unloading

Loading and
unloading

Loading and
unloading

Processing

Processing


Processing
Process, waste
treatment
Waste  treatment
Waste  treatment
Waste  treatment
 Waste treatment
 Principal Hazardous Materials

 Fuel and lubricating oils, asphalt, oil additives, inorganic acid and
                 caustic
 *
 Old refinery used as storage and distribution facility primarily

                                          120

-------
REQUIRED  OR USED  BACK-UP SYSTEMS
Valving or  pumping system required
to make this  fail-safe
 Disposal  system required
 Curbing and drainage system required
                                         PLANT C (Continued)
REMARKS
                                        Fire regulations require diked storage
                                        Present system is inadequate and must be replaced.
                                        Approach is thought to be valuable if system accuracy
                                        can be improved.  Probably detects large leaks.
                                        Is fail-safe only to extent used by operators.
                                        In experimental stage, believed to give tanker personnel
                                        false sense of security^-not connected to shut-off system
                                        Prevents release of product to waterway
                                        Detects  leaks  in heat exchangers; requires diversion
                                        system and  catch basins in event of accident
                                        Detects  leaks but not fail-safe
                                         Not fail-safe,  but  prevents most accidents in
                                         plant  discharge from reaching waterway

                                         Allow  two  levels of treatment and different
                                         separation and  treatment  techniques

                                         Detects overloading of  separator and prevents direct
                                         release of oil  into clean waste treatment facility
                                               121

-------
     DESIGN CRITERIA. EQUIPMENT. AND PROCEDURES USIil)  IN PLASTICS AND RUBBER FACILITY  -  PLANT
                                 ITEM

I.   Dikes Around Individual  tanks or groups oi  tanks


2.   Separator pits  for draining tanks
                                                               TYI'K
Design crltorlu,    Process,  slor«K«'
equipment

Design criteria,    Process
equipment
3.  First half hour of heavy rain runoff flows into
    trade waste system for processing in water
    treatment area
Procedure
                                                                                   Process, storage
4.  Lagoon for diversion of one day's trade waste
    for further processing

5.  Other lagoons for diversion and storage of
    2-3 days'  wastf.

6.  Sight glasses on tanks

7.  Written handling procedures for loading and
    unloading tanks
8.  Level or pressure alarms on critical tanks
Design criteria     Waste treatment
Design criteria     Waste treatment
Equipment

Procedure



Equipment
Process

Storage, process
loading and unload-
ing

Transfer, process
9.  Piping above ground with concrete ditches
    underneath
Design criteria,    Transfer
equipment
10. Operator on duty in waste treatment area
    24 hours a day

11. Concrete ditches surrounding tank car unloading
    area

12. Hard surfaced areas near loading and facilities
Procedure


Design criteria,


Design criteria
13. Gravity overflow lines on tanks'


Principal Hazardous Materials:  Butadiene, Styrene, Latex, Rubber Formulations.
Design criteria,
equipment
Waste treatment
Loading and
unloading

Loading and
unloading

Loading and -unload-
ing, process
                                                 122

-------
                           PLANT D (Continued)
REQUIRED OR USED BACK-UP  SYSTEMS

Requires control of valves  and lines
going through dikes

Requires system for disposal of
material collected  in pits
Requires separate  storm and process
waste system
REMARKS
Used whenever tanks are being
cleaned ;or as an overflow
protection measure

Used to collect any oil or wastes
that would be washed off in heavy
rain; one half hour may be
insufficient
 This  is  a back-up for waste treat-
 ment  system

 Requires operator's use
 Requires appropriate maintenance
 and checking
                                           Used when load on waste  processing
                                           is heavy or failure in system
                                           Not fail safe, but may help to
                                           prevent spills
                                           Ditches empty into trade waste,
                                           and are used to collect any
                                           spills from pipes

                                           Operator  is able to divert flows
                                           or spills
 Requires adequate waste treatment
 or disposal system

 Requires collection system as
 described above

 Requires sumps or holding vessels
 for overflow
 Overfilled tanks  release
 material by gravity  flow  to  sump
 or tank instead of spillage
                                     123

-------
DESIGN CRITERIA.  EQUIPMENT AND PROCEDURES USED IN PETROCHEMICAL AND CHEMICAL  f^f!TLTTY - PLANT,E
                                  ITEM
 1.  Dikes around most storage tanks
2.  Sui.ips or traps with eductors inside diked area
3.  Excess flow valves on critical lines used during
    transfer

4.  At  least one catch basin or holding tank in each
    process waste stream

5.  Skimmers in storm sewer runoff stream
TYPE

Design criteria,
equipment

Design criteria,
equipment

Equipment
Design criteria,
equipment

Equipment
AREA

Process,
storage

Storage
Loading and unload-
ing

Process, waste
treatment

Waste treatment
 6.   Concrete barrier around hazardous materials tanks     Design criteria,    Process, storage
                                                          equipment
 7.   Sumps  with eductors  in concrete barrier tanks
Equipment
Process, storage
 8,   Level  alarms on selected  tanks
Equipment
                                                                              Process
 9.   Operator  in control room 24 hours per day             Procedure

 10.  Feed  line pumps of critical materials can be shutoff  Equipment
     by  scales under tank cards or process vessels

                                                          Design criteria,
 11.  Separators, sumps, and process sewers used to collect equipment
     spills  in loading areas

 12.  Return  lines on loading of cars goes to separate tank Design criteria,
                                                          equipment
 13. Planned  inspection of hoses and piping
Procedure
                    Process

                    Process,  loading
                    and unloading
Process, loading
and unloading

Loading and
unloading

Storage, transfer
 14. Rigid connections on materials of high hazard
Equipment
Loading and
unloading
                                              124

-------
                           PLANT E  (Continued)
REQUIRED OR USED BACK-UP SYSTEMS

Sumps or valves in  lines passing
through dikes required

This is a back-up system for dikes
Requires operators  to observe use of
system
REMARKS
Spills in diked areas cannot flow
out under gravity

If flow is too large due to tank
or line failure, flow is shutoff

A safety measure to prevent heavy
loading of waste treatment system

Planned to remove any hydrocarbons
from runoff water

Used primarily as a safety measure
around very flammable and hazardous
materials
 Is  a back-up system to prevent gravity
 flow of spilled materials
                                           Used mostly  for flammable or hazard-
                                           ous materials
 Back-up for alarm system
 Is a back-up system for transfer  of
 fluids

 Is a back-up system during  filling
 operat ions
                                           Used  primarily  in  transfer of very
                                           hazardous materials  to prevent over-
                                           filling
 Gravity  flcv "•••' ••  '
 tanks

 Normal plant practice with extra
 attention given to hazardous materials
 lines

 Eliminates problems  of  flexible lines
                                     125

-------
 DESIGN CRITERIA, EQUIPMENT AND PROCEDURES USED IN PETROCHEMICAL AND CHEMICAL  FACILITY
                                 PLANT E (Continued)
                                 ITEM
15.  Use of atmospheric  pressure  and  vacuum systems  to
    convey materials  rather  than pumps

16.  Curbing around selected  process  areas
TYPE

Design criteria,
equipment
AREA

Loading and
unloading
Design criteria     Process
Principal Hazardous  Materials:   Chlorine, Alcohols,  Olefins,  Sodium,  Flammable Materials.
                                         126

-------
                          PLANT K  (Contitiued)
REQUIRED OR USED BACK-UP  SYSTEMS          REMARKS
                                           Believed to  reduce potential for
                                           spills during  transfer operations
Is a back-up system  for small spills
in process area
                               127

-------
 DESIGN CRITERIA. EQUIPMENT AND PROCEDURES USED IN REFINERYAND STORAGE AND DISTRIBUTION FACILITY

                                           PLANT F
                               ITEM
 I.  Separate storm water and process water systems
2.  Four large guard basins to retain storm water
3.  Dikes around selected tanks
    Separate drainage system for diked tanks
5   Emphasis on placing responsibility for spills on
    operator
 TYPE

 Design criteria,
 equipment

 Design criteria,
 equipment

 Design criteria,
 equipment

 Design criteria,
 equipment

 Procedure
                                                                               AREA
Process
Waste treatment
                                                                               Storage
Storage
6.  Cathodic protection of pipelines, frequent corrosion   Design criteria,     Transfer
    inspection                                             procedure

7.  Testing and certification of hoses at loading dock     Procedure           Loading and
    on regular basis                                                           unloading

8.  Use of articulated swivel joint steel loading arms     Equipment           Loading and
    on increasing level                                                        unloading

9.  Gravity flow of oil for first half hour to check       Procedure           Loading and
    connections before applying pump pressure                                  unloading

10. Low pressure shutoff on selected lines                 Equipment           Transfer
11. Drip pans at appropriate loading points                Equipment


12. Securing of normally closed lines (valves)  by seals    Procedure
                    Loading and
                    unloading

                    Process, loading
                    and unloading,
                    storage
13.  Small local tanks of acid or caustic to help in
    neutralization
Equipment, design   Process, waste
criteria            treatment
                                               128

-------
                           PLANT F (Continued)
REQUIRED OR USED  BACK-UP SYSTEMS
Must have method  to divert flow into
these basins
This  is a  back-up system to separate
material released in diked areas
REMARKS

Design to separate oily wastes
from water runoff

Designed for holding storm water
or spills for further treatment

Dikes used depending upon
flammability of material
                                           This is an attempt to make
                                           employees more aware of the  con-
                                           trol and consequences of spills
Requires manual check for leaks, drip
pans,  etc.
Plant staff believe these are safer
than flexible hoses

Used to help spot leaks when under
low pressure and prevent large leaks

Used to detect if there is a leak in
pipeline
 Need curbs or dikes around tanks
This is planned to eliminate
accidental opening of drain lines,
dike feed throughs, etc. which could
result in spills

Used to help neutralize on site small
spills
                                   129

-------
DESIGN CRITERIA. EQUIPMENT AND PROCEDURES USED IN REFINERY AND STORAGE AMD DISTRIBUTION  FACILITY


                                      PLANT F (Continued^
                                   ITEM
                                                          TYPE
  14.  Continuous monitoring of waste water  system  for pH   Equipment
      at  several points
  15.  Hard  surfaces  in process areas

  16V  Above grade  product  lines over drainage ditches


  17.  Gauging manifolds  on tanks



  Principal Hazardous Materials;  Oil, Hydrocarbons.
Design criteria

Design criteria


Equipment
AREA

Waste treatment


Process

Process, transfer
Storage, loading
and unloading
                                             130

-------
                            PLANT F (Continued)
REQUIRED OR USED BACK-UP SYSTEMS

Requires system for monitoring of
other substances as well
REMARKS
                                           Drainage  goes  to waste treatment
                                           system

                                           Permits rapid  measurement of tank
                                           levels during  transfer operations
                                     131

-------
CRTTERL
PROCEDURES AND EQUIPMENT IN PETROCHEMICAL AND CHEMTCAT.  FACILITY -_
                 ITEMS
   1. Separate chemical sewer and clean water storm          Design criteria
     sewer drainage systems.


   2. Rainwater collection and holding pond to contain       Design criteria,
     first fifteen minutes of runoff;  the remainder        procedure
     being diverted directly into waterway.
   3  Practically all piping is above ground.                Design criteria
  4.  Regular  periodic  inspectirn using standard pro-        Procedure
      cedures  for all piping  including hydrostatic
      testing  and visual  inspection.
   5. Normal activities of plant operation requires          Procedure
     operators  to observe or at least walk along some
     of  the exposed pipelines during their daily
     activities.
   6. .Long  interfacility  liquid transfer pipelines           Design criteria,
      supplied with  check valves, and emergency  liquid       equipment
      storage tanks  at both ends.
   7.  Standard  procedures established  for communicating       Procedure
      via  telephone between both ends  of long major inter-
      facility  pipelines.
                                     132

-------
                        PLANT G  (Continued)
AREA

Process, other



Process, other
REQUIRED OR USED
BACK-UP SYSTEMS
                              REMARKS
Backup system to insure chemical
spills do not get into the rainwater
discharge from the facilities.
Requires means for
detection of chemicals
or contaminants  in rain-
water runoff diverted
directly to waterway.
Collects the potentially
dirty initial rainwater run-
off which has washed old
spills of chemicals from
processing areas,  etc.
 Process,  other
 Transfer,  other
 Transfer, others
 Transfer
 Transfer
 This is a backup
 system for the
 preceding item.
                              Permits  immediate  visual  de-
                              tection  of leaks  or  spills
                              associated with transfer  pipe-
                              lines.

                              Primary  purpose is to prevent
                              accidents--built-in  spill
                              prevention and detection
                              aspects.

                              Certain sample points or  data
                              taking points are stratically
                              located in plant, such that
                              operators must regularly visi:
                              these points--requiring their
                              visual observation of pipe-
                              lines arid other equipment
                              enroute.

                              In case  of emergency, the en-
                              tire contents of the trans-
                              fer pipeline can be  emptied
                              into a storage tank at either
                              end of the pipeline.
                                   133

-------
.DESIGN  CRTTi:j;_A.  PVOi;:_M.i;.__..  .' iOj:O!:-'nM''NT IN PETROCHKMICA1. AND CHEMICAL  FACILITY -
                        ITEMS
       8. All moves of liquid through  large major  inter-
          company transfer pipelines made in increments or
          "batches", utilizing transfer tanks  located at
          both ends of pipeline.

       9. Areas under transfer pipelines have  concrete
          surface.

      10. Loading racks at loading  terminal are mounted
          over concrete surface.
TYPE

Proceduie,
equipment
Design criteria
Design criteria
      11. Education program aimed at  process unit  op-
          erators  to make  them aware  that  they have  the
          ultimate responsibility for spills.
Procedure
      12. Sample lines purged into collection drums.
Procedure
          LPG storage tanks equipped with high-pressure
          alarms.
Equipment,
design criteria
      14. LPG pumps equipped with high-flow  cutoff.
      15. Many storage tanks are surrounded by dikes.
Design  criteria,
equipment

Design  criteria,
equipment
                                        134

-------
                          PLANT G (Continued)
Transfer,
processing

Loading and
unloading.
Process, others
Process
                    REQUIRED OR USED
                    BACK-UP SYSTEMS

                    Requires gauging of  liquid
                    levels in  receiving tanks
                    and transfer  tanks.
Grade, curbing, and
drainage system required.

Curbing, grade, and
drainage system required.
Records maintained by
company for each employee,
showing record of spills
caused by each employee;
poor record can result  in
official reprimand, time
off without pay, or loss of
job.

Collections and disposal of
liquids from  purged waste
liquid collection drums.
                             REMARKS

                             Close control provided over
                             quantities moved, with in-
                             ventory control providing
                             direct indication of spills.
Any liquids lost in this
area of high-spill potential
and frequency are directed
to containment rather than
being allowed to escape.

This philosophy gives promise
of being an ultimate "fail-
safe" procedure for prevent^n
spills.
This replaces the old system
of purging sample lines
simply onto the ground or
processing pad.
Storage
Storage,
transfer

Storage
Requires attention of
operator, and  subsequent
appropriate corrective action.
Requires proper dike drain-
age system operation to  in-
sure impounding of  spills,
and the proper transfer  to
waste disposal of the  con-
tained spill.
Dikes are required by fire
regulations, but also serve
as an effective "fail-safe"
spill prevention measure.
                                     135

-------
 c;iiu:u].\.  PROCKIH'RKS AND EQUIPMENT IN PF.TKOCHHMTCAL  AND.CHKMICAI,,  FACILITY

                        PLANT G (Continued)
                  ITEMS                                    TYPE

16.  Some storage tanks are equipped with high-             Design  criteria,
    level alarms.                                          equipment

17.  Manual tank gauging occurs regularly.                  Procedure
18. A log is maintained which indicates the con-            Procedure
    ditijn (open or closed) of each valve on the
    drain lines from dikes surrounding storage tanks.
19. Large impounding area provided for tvbltting- of -''^r
    any large spills of chemicals which would  drain         Design criteria
    from the plant at a rate higher than the maxi-
    mum which the waste treatetnent facilities  could
    handle.
20. Process areas handling the most hazardous ma-           Design criteria
    terials from a pollution viewpoint are completely
    surrounded by dikes, drainage ditches, etc. and
    are provided with specific waste treatment
    facilities designed specifically for  those
    materials being handled.

21. Loading arms are washed with a minimum quantity         Procedure,
    of solvent wnicfi is collected in containers             equipment
    oC: i'-:ic.tea for used solvent for collection
    and >: i ?posa 1 ,
                                   136

-------
                           .PLANT  G  (Continued^
                    REQUIRED OR USED
                    BACK-UP SYSTEMS
                                                  REMARKS
Storage
Storage
Waste treatment
Process
Loading and
unloading
Manual gauging  provides
a back-up  for the  tanks
with continuously
monitored  liquid
level indicators
This is a backup
system for  the main waste
treatment facilities
The main waste  treatment
facilities of the  plant
provide backup  for  the
specialized waste  treat-
ment facilities  serving
the hazardous process area
Regular collection of waste sol-
vent and transportation to waste
disposal facilities required
This procedure was developed
to provide better control
over the position of drain
valves from dikes which should
be in the normally closed
position such that any spill
will be impounded' behind the
dike, and can later be
drained under control to waste-
treatment or product recovery
areas.

After a large spill was col-
lected and impounded, it could
be fed back to the waste trea-
ment facility at a rate that
would not exceed the waste
treatment facility's capacity
during normal plant operation

An example of such a system
is one in which phenol is
processed.
                                     137

-------
DKST.CN CRITERIA. PROCEDURES AND EQUIPMENT IN PETROCHEMICAL AND CHEMICAL  FACILITY -


                             PLANT G(Continued)
                         ITEMS                                     TYPE

       22. All  sewers  sampled at  least  onre a  day.                 Procedure
          Chromotography used  to  identify each  specific
          chemical  in the sewer  system.
       23.  Suction  trucks  are  used  to  remove waste  chemicals       Procedure,
           collected  in  sumps  during equipment  "turn-around".      equipment
       Principal  Hazardous Materials;   Chlorine,  Organic  Solvents,  Phenol
                                     138

-------
                         PLANT G  (Continued)
                    REQUIRED  OR USED
AREA                BACK-UP SYSTEMS              REMARKS

Process,            This  is a backup system for  The presence of any organic
other               the various monitoring and   products in excess of the
                    detection procedures and     acceptable limits set by the
                    systems used to identify     company is traced to the
                    spills in processing         specific operator responsible
                    storage and other areas.
 Processing,          Regular chemical sewer       Waste materials from equip-
 other                system and waste treat-      ment cleaning operations are
                     ment facilities.             removed in a concentrated
                                                  form, thereby facilitating
                                                  disposal.
                                    139

-------
DESIGN CRITERIA! EQUIPMENT AND PROCEDURES IN REFINERY I  OIL STORAGE j  AND DISTRIBUTION FACILITY
                                         PLANT H
                      ITEM

        1.  Drainage Ditches or Dikes around
            entire plant site
     TYPE

Design Criteria,
   Equipment
 AREA

  all
        2.  Storage tank diked—diked to
            1257, of capacity

        3.  Drainage from diked areas, process,
            and plant go to retention basins

        4.  Wastewater treatment plant for all
            water streams leaving plant
        5   Retention basins
               (a)  Normal

               (b)  Excess
Design Criteria
Design Criteria,
Procedure

Design Criteria,
Equipment,
Procedure
Design Criteria,

Procedure
Storage
                         all
 Waste
Disposal
  all

  all
        6.  Loading areas drain to wastewater
            treatment plant
Design Criteria,       Loading
Procedure
         7   Company owned boom for barge!     '-
            loading area

         8.  Curbed process areas
Procedure
Design Criteria
Loading
Process
        9.  Articulated Loading Arms
Equipment
Loading
         10.  Process  piping on racks


         11.  Standby Wastewater Transfer
             Pumps
Design Criteria        Process,
                    Transfer,Loading

Design Criteria,     Waste  Disposal
    Equipment
         12. Development of plant water
            recycle  system
 Procedure
                                                                                all
         Principal Hazardous Materials:

         Petroleum Products  from Crude Through  Refined Acids, Phenols, Heavy Metals
                                          140

-------
                        PLANT H (Continued)
   REQUIRED OR USED
   BACK-UP SYSTEMS

All drainage leads to
holding basins
                REMARKS

  Serves  to insure that  internal  plant
  spillages are not removed  beyond
  property line
Holding basins and plant per-   Dikeage  required for  safety  reasons
imeter dikes & ditches used
Plant perimeter dikes  and
ditches used

Retention basins required
  Requires all water to go through
  wastewater treatment plant

  Plant employs physical and  chemical
  separation processes for removal
  of pollutants
 Excess basins  &  perimeter
 dikes and  ditches used
 Perimeter  dikes  & ditches
 used
 Retention  basins  required
Drains  to wastewater
treatment plant  required

Drainage to wastewater
treatment plant  required

Drainage systems
  Holds normal run-rff and  surges

  Diked area around two tanks  is used
  to, receive excess storm drainage via
  pumping

  Meets plant operational philosophy of
^treating all water emissions regardless
  of source

  Part of industry-government  group
  under National Contingency Plan

 Normal  design  criteria  to prevent spread-
 ing and to  direct flow  to treatment facility
  Ease of leak detection,  repair,
  renovation

  Since all water streams  leaving  plant
  area must be pumped, good operational
  practices dictates spares

  To minimize overall water usage  and
  improve efficiency of usage
                               141

-------
              ITEM

1.   Elimination of drains  in areas
    handling highly toxic  chemicals

2.   Batch collection and treatment
    cf all water streams
     TYPE

Design Criteria,
   Procedure

Design Criteria,
   Procedure
  AREA

Process


All
3   In old plants,  sealing of all
    area drainage sewers

4.  Diking of tanks
Procedure
Design Criteria
 All
Storage
5.  Discharge of treated wastewater
    to municipal sewers
Procedure
 Waste
Disposal
6-  Designation of specific employees
    to discharge treated waters
 Procedure
 Waste
Disposal
7.  Roofing of'areas where spills
    might occur
Design Criteria
Transfer,
Loading &
Unloading
8.  Waste sludge disposal by regula-
    tory agency approved contractors
Procedure
 Waste
Disposal
9.  Company program for education of
    operating personnel
Procedure
General
Principal Hazardous Materials:   Paints,  Solvents,  Cyanides,  Heavy Meals, Oils
                                  142

-------
                     PLANT I  (Continued)
REQUIRED OR USED
BACK-UP SYSTEMS


Manual removal  and
disposal required
Wastewater  treatment
system required

Wastewater  treatment
system required
 Wastewater treatment
 system required
 Regulatory agency
 approval
              REMARKS

 Most positive method for containment
 and treatment

 Small volume of wastewater streams per-
 mits collection & treatment to degree
 required for emission

 Only practical method to insure
 col lection

 Done on a selective basis—prefer to
 depend upon drainage & collection to
 central water treatment system

 Company policy to treat to level accept-
 able to municipal sewage system in order
 to insure that additional treatment is
 given before emission

 Assigns responsibility for insuring that
 quality of treated wastewaters meets
 established standards
. i
 Objective is to insure that storm water
 drainage does not remove spilled sub-
 stances since it is more economical to
 provide roofing than large wastewater treat-
 ment plant capable of handling storm water
 flows

 Company will not contract with unlicensed
 disposers because of contingency liability
 possibilities

 Company believes that operating personnel
 must be made aware of the consequences
 of leaks and spills
                                   143

-------
DESIGN CRITERIA, EQUIPMENT AND PROCEDURES IN CH8MICAL FACILITY - PLANT J
            ITEM

1.  Large number of separated
    process units

2.  Prohibition of certain pro-
    cessing operations at plant
     TYPE

Design Criteria,
Procedure

Procedure
                                                                     AREA
3.  Extensive sewer system equipped
    with automatic recording instru-
    mentation
Design Criteria,
Procedure
   all
4.  Diked tanks
Design Criteria
Storage
5.  Holding basins and lagoons
Design Criteria,
Procedure
 Waste
Disposal
    Primary and secondary waste-
    water treatment plant
Design Criteria,
Procedure
 Waste
Disposal
    Random program of monitoring
    the effluents from individual
    process areas
Procedure
  All
8.   Curbed process areas
Design Criteria
                                                                   Process
                                  144

-------
                        PLANT  J  (Continued)
REQUIRED OR USED
BACK-UP SYSTEM
                                         REMARKS

                       Segregation permits greater attention to  problems
                       peculiar to a particular process.

                       The hazardousness of certain products is  regarded
                       as  so great that incorporation of adequate  safe-
                       guards at this location is infeasible.

                       Selected points in process sewer system are ana-
                       lyzed on short-time repetitive schedule for car-
                       bon containing or oxygen demanding substances.
                       Results are electronically recorded in central
                       control.  System provides alarms and causes actions
                       to  be initiated'
 Collection system     Dikes are provided on a selective basis.   However,
 and wastewater treat- because of plant experience wherein a  tank rupture
 ment  plants required  washed out a dike, plant relies on area   ditches,
                       & peripheral dikes to prevent spread beyond plant
                       borders.
Wastewater
treatment
plant required.
Wastewater  treat-
ment  plant
Wastewater  treatment
plant required
                       Large  volume basins  are maintained  into which
                       "slugs" of spilled substances  can be  routed for
                       purposes of dilution and for protection of bio-
                       logical wastewater treatment plant.

                       Plant  can be operated in many  different modes, is
                       equipped with monitoring & control  instrumentation,
                       operated by trained  personnel,  & protected against
                       upsets by the use of holding basins & lagoons to
                       which  slugs of hazardous polluting  substances can
                       be  sent.

                       A highly visual sampling station installed on a
                       random schedule on sewers from processing areas
                       results in encouraging operating personnel to
                       improve housekeeping,  reduce leaks, and decrease
                       load to wastewater treatment plant  since they
                       know that record is  being obtained.

                       Good operating procedures to confine  leaks and
                       spills to desired channels.
                                 145

-------
         r.RTTKRTA,'  EQUIPMENT AND PROCEDURES  TN CHEMTCAL FACTLTTY -  PLANT J (Continued)
                       ITEM

          9.  Plant wide spill reporting
              system
   TYPE

Procedure
  AREA

All
          10. Independent Pollution
              Control Group
Procedure
General
           11. Plant safety—Pollution
              Control Educational Program
Procedure
                     General
Principal Hazardous Materials:  Large Variety of Reactive Organic and Inorganic Chemicals
                                       146

-------
                             PLANT J (Continued)
REQUIRED OR USE1)
BACK-UP SYSTEM

Flexible waste-
water treatment
system required.
                  REMARKS

Special telephone and alarm system is available
for reporting spills and leaks.  Employees are
trained in its use & are subject to disciplinary
action for failure to report unless protection
of life & property takes precedence.

Through the establishment of a pollution control
group reporting to top management, area manage-
ment can be judged on the effectiveness of pol-
lution control efforts.  Group has authority to
require periodic reviews of water usage & reviews
all changes & additions in processing sites.

Plant management has established a direct correla-
tion between safety record and pollution control
record for operational areas.  Consequently, edu-
cation and training of plant personnel in both
areas is carried on continuously.  Furthermore,
records show that wastewater plant pollution load
is decreasing even though overall plant production
is increasing.
                                  147

-------
DESIGN CRITERIA.  EQUIPMENT AND PROCEDURES USED IN REFINERY. STORAGE AND DISTRIBUTION FACILITY! PLANT J<
                                 ITEM
1,  Plant graded toward drain system
                                                               TYPE
                                                                                   AREA
Design criteria      process
2.  Waste process system separate from water runoff system     Design criteria
3.  Overflow and emergency basins for holding heavy rain
    and emergency spills

4.  Scheduled startup, maintenance and shutdown of storage
    and process areas done with area drains blocked
Procedure
                    Process,  storage,
                    loading  and
                    unloading
Design criteria     Waste  treatment
Storage, process
5.  Planned inspection and replacement of pipelines, equip-    Procedure
    ruent, etc.
                    Storage, process
                    transfer
6.  Specific trainee programs with oral and written exams
    for operator status

7.  Check sheets used for many transfer and process
    operations

8.  Daily check of pipelines from wharf to plant

9.  Selected storage within concrete diked area
Procedure


Procedure


Procedure

Design criteria
Process, loading
and unloading

Process, loading
and unloading

Transfer

Storage"
 10. Oil spill booms available on dock
 11. Low dikes used in storage areas when more than one tank
    within a common dike

 12. Rainwater accumulated and drained sequentially from
    diked areas using manually actuated valves
Equipment
Design criteria,
procedure
Loading and
unloading
Design criteria     Storage
Storage
13. Automatic level measurement systems widely used
Equipment
Process, storage
14. Trailer loading facility graded toward hold tank
                                                 148
Design criteria     Loading  and
                    unloading

-------
                           PLANT K (Continued)
REQUIRED OR USED BACK-UP SYSTEMS

Adequate waste  treatment system
required
REMARKS
This  is a back-up system for all
spills

Requires checklist to insure drains
unblocked at  end
Separate treatment of selected
streams before combining process
wastes

Five-day total retention based on
worst 30-year rainfall is provided

Plant experience indicates spills
occur during startup, maintenance
and shutdown.  This helps contain
spills during these times

Specified replacement dates and
X-ray, dye technique inspection
provided
 Requires  controlled use of check
 sheets
This is an attempt to get operators
more responsible for spills
 Requires proper use of booms
                                           Tanks very near water course are
                                           diked by concrete barriers

                                           Not fail safe but a control measure
                                           Used to contain limited spills and
                                           rainwater

                                           Prevents overloading water treat-
                                           ment system; manual valves normally
                                           closed

                                           Central control stations with
                                           operators can monitor tank levels
                                           regularly
                                   149

-------
DESIGN CRITERIA. EQUIPMENT AND PROCEDURES USED IN REFINERY. STORAGE AND DISTRIBUTION  FACILITY

                                  PLANT  K (Continued)
                                 ITEM
15. "Meter Loading" of trucks with calibrated meters
Principal Hazardous Materials:  Oil, Hydrocarbons.
TYPE
Procedure
AREA

Loading and
unloading
                                           150

-------
                               PLANT K  (Continued)
REQUIRED OR USED BACK-UP  SYSTEMS
REMARKS

Helps to prevent spill by transferring
limited amounts
                                          151

-------
          DESIGN CRITERIA. EQUIPMENT AND PROCEDURES USED IN CHEMICAL   FACILITY -
                                 ITEM

1.   Acid and caustic tanks and loading areas have
    individual catch basins to hold stored capacity

2.   All oil process areas have sewer system leading to
    trap and skimmer

3.   Double capacity trap for oil operations
4.  Cooling towers replacing once through process  water
TYPE                AREA

Design criteria,    Storage
equipment

Design criteria,    Process
equipment

Design criteria,    Process
equipment

Design criteria,    Process
equipment
5,  Paved process areas to control  runoff
Design criteria    •- Process
6.  Hourly visual inspection of oil collection trap
Procedure
                    Waste treatment
7.  High level alarms on indoor tanks

8.  Overflow lines on outdoor storage tanks
9.  Oil tanks within common dike;  acid and caustic tanks
    have separate dikes

10. Dikes drained by pump out rather than gravity
Equipment

Design criteria,
equipment

Design criteria
Design criteria
Process, storage

Process, storage


Storage, process


Storage, process
11. Rail tracks and truck loading areas  sloped toward
    drain system
Design criteria
12. Tank car valves routinely checked before and after     Procedure
    loading and unloading

13. Specific procedures for transfer operations  with check Procedure
    lists
Loading and
unloading

Loading and
unloading

Process loading
and unloading
Principal Hazardous Materials;   oil Detergents,  Soaps.
                                                152

-------
                        PLANT L (Continued)
REQUIRED OR USED BACK-UP  SYSTEM ft
REMARKS
Requires  some  separation and treat-
ment of process  water
Waste water  collection and treatment
required
 Requires drainage system for overflow
 This  is a back-up system for spills
 into  dikes

 Adequate drain sys tern required
Frequent spills occurred from leaks
into process water and into water
course
                                           Inspection performed so  that  diver-
                                           sion can be accomplished

                                           Primarily a safety measure
                                           Primarily due to plant siting
                                           requirements
                                           plant staff feels that this is
                                           most important in preventing
                                           spills
                                   153

-------
      DESIGNCRITERIA,  EQUIPMENT AND  PROCEDURES  USED  IN METAL  PRODUCTS   FACILITY - PLANT M
                                 ITEM
1.   Separate  sewer  system for waste  acid
                                                            TYPE
Design criteria
2.   Neutralization or  removal  (by hauling)  for acid streams  Design criteria,
                                                            procedure

3.   Oily waste separated  in API  separators  and trucked away  Equipment,
                                                            procedure
4.  Oil skimmers  on all main plant water ditches
Equipment
5.  Acid tanks  placed  in  concrete dammed area with drain     Design criteria
    to acid sewer
6.  Gravity loading of  acid  trucks


7.  Hard surface  truck  loading  acid area
Design criteria,
procedure

Design criteria
8.  High level alarm in  sump used  in acid storage area       Equipment
AREA

Process, waste
treatment

Process, waste
treatment

Process
Waste treatment

Process, waste
treatment

Process, storage
Process, loading and
unloading

Process, storage
9.  Automatic pH  control  of effluent
Equipment
Waste treatment
    Principal Hazardous Materials;  Acid, Caustic, Oil and Oily Waste.
                                                154

-------
                          PLANT M (Continued)
REQUIRED OR USED BACK-UP  SYSTEMS
                                           REMARKS
Requires adequate  waste  oil  separation
system

Same  as above
 This  is  a back-up measure to detect
 unusual  acid leaks
                                           Metal acid wastes  are  trucked away;
                                           relatively clean acids  are neutralized
                                           Designed to prevent  spills  during
                                           pumping operations
                                           Required because of acid  content  of
                                           waste streams
                                    155

-------
     DESIGN CRITERIA  PROCEDURES AND EQUIPMENT USED IN STORAGE AND DISTRIBUTION  FACILITY
                                         PLANT N
                               ITEM
 .   All tanks  within  common  dike
2.  Shutcff valves  up  and  downstream of pumps
3.  Sampling of all cargoes  prior  to unloading
4.  Blow back of flexible  hoses  to ship
5.  Hard surface transfer  areas
TYPE

Design criteria,
equipment

Design criteria,
equipment

Procedure
                                                        Procedure
Design criteria
                                                                             AREA
Storage
Storage, loading
and unloading

Loading and
unloading

Loading and
unloading

Transfer, loading
and unloading
6.  Blending and canning  operations  inside diked area    Design criteria     Process
7.  Dip stick gauging is  standard
8.  Drainage valves on dikes
Procedure
                    Storage, loading
                    and unloading
Design criteria     Storage
Principal Hazardous  Materials;  Xylene, Toluene, Glycol, Agricultural and Organic Chemicals.
                                           156

-------
                             PLANT N (Continued)
REQUIRED OR USED BACK-UP SYSTEMS
REMARKS
This is a back-up system to
prevent accidents.
Small facility with tanks next to
each other

Helps prevent spills at pumps--
a frequent occurrence

Also used to maintain product
quality

Prevent spills during disconnect-
ing lines
                                           Spills are common in blending
                                           operations but are small

                                           Poor experience with level gauges
                                           suggests this approach is better
                                     15"

-------
                        JRES  AND EQUIPMENT USED IN REFINERY. STORAGE.  AND PETROCHE>"^At. FACILITY
                                           PLANT  0
                                 ITEM
1.  Process areas are sloped toward plant ditch system

2.  Separate collection system for phenols,  sulfidep,
    ammonia, etc.
TYPE

Design criteria

Design criteria,
equipment
AREA

Process

Process, waste
treatment
3.  Oily waste streams flow into closed drain system to
    central oil-water separator

4.  Clean process water and treated water go  to large
    holding basins

5,  Petroleum tanks diked with concrete dikes in process
    area and earthen dikes elsewhere

6.  Water drains in dikes open only during rain periods
    and checked every two hours

7.  Elevated transfer piping with regular inspection
    procedures

8.  Overpressure relief valves on transfer lines
Design criteria,
equipment
Process, waste
treatment
Design criteria     Waste treatment
Design criteria
Design criteria,
procedure

Design criteria,
procedure

Equipment
Storage and
process

Storage
Transfer
Transfer
9.  Automatic shutoff valve system with liquid  level
    gauges
10. Transfer areas for truck and  rail  loading sloped
    toward drains

11. Tank car wash water goes through oil  separator
12. Scupper plugs on tankers  and  barges
13. Flexible hoses  being replaced  by metal  loading arms
14.  Catch basins  used on ships  under  connections
15.  Lines either drained  back to  ship  or  pumped  out  before
    disconnect
                                                 15R
Design criteria,
equipment
Design criteria


Equipment


Equipment


Equipment


Equipment


Procedure
Transfer, storage,
loading and unload-
ing

Loading and
unloading

Loading and
unloading

Loading and
unloading

Loading and
unloading

Loading and
unloading

Loading and
unloading

-------
                         PLANT 0  (Continued)
REQUIRED OR USED BACK-UP  SYSTEMS
REMARKS
                                           This is a reclamation system which
                                           acts to prevent discharge  of these
                                           materials
This is a back-up  system for all
spilled materials.
Three to five week holdup times in
large basins

Diking due to local fire codes
Careful checking required to make
fail safe.
Requires method of collection of
vented  substances.
                                           System now being installed  based
                                           upon good experience at other
                                           locations
                                           Better experience obtained with
                                           metal system
                                           Procedure depends upon elevation of
                                           ship and wharf
                                    159

-------
DESIGN CRITERIA.  PROCEDURES.  AND EQUIPMENT USED IN REFINERY. STORAGE. AND PETROCHEMICAL FACILITY -
                                     PLANT 0  (Continued)
                                 ITEM
                                                               TYPE
16. Written instruction to ship personnel before unloading     Procedure
17. Written procedures and check sheets used for all
    transfer operations

18. Cleanup truck on standby during repair operations
19. Employee motivation program aimed at reducing spills
    and keeping oil from water
Procedure
Procedure,
equipment

Procedure
AREA

Loading and
unloading

Loading and
unloading

Process, loading
and unloading
Principal Hazardous Materials;  Oil, Phenol, Acid, Caustic,  Petroleum Products and Derivatives.
                                              160

-------
                              PLANT 0 (Continued)
REQUIRED OR USED BACK-UP  SYSTEMS
REMARKS
                                           Language  problems have resulted in
                                           past  spills
Not fail  safe,  but  a backup for
other equipment
                                           Believe that  employee  training and
                                           motivation is essential  to prevention
                                           program
                                     161

-------
DESIGN CRITERIA,  PROCEDURES AND EQUIPMENT IN METAL PRODUCTS. FACILITY -_
                 ITEMS                                        TYPE

      1.  Many  storage  tanks  surrounded by dikes                Design  criteria,
                                                              equipment
      2, Manual  tank gauging occurs regularly                  Procedure
      3. All  underground  fuel storage tanks are                Design  criteria,
        equipped with mechanical-type internal                equipment
         liquid  level sensing devices with above-
        ground  visual indicators

      4. The  ground covering all of  the buried                 Design  criteria
        storage tanks is graded s-ich than any spills
        above ground will be directed into the
        waste water treating system.

      5. A  single sewer system handles all rain-               Design  criteria,
        water runoff as well as any spills of liquids         equipment
        from the processing, manufacturing operations,
        or storage tank  farm areas.
      6. All  areas  in which solvents, cutting oils, and        Design  criteria
        acids are  used are provided with appropriately
        sloping hard surfaced floors, and curbing,
        which will direct any spill to a sump from which
        it  is pumped either  into a storage tank for re-
        processing, or disposal.
      Principal  Hazardous Material^:  Oil, Acid Washes, Metal  Treatment Chemicals.
                                     162

-------
                           PLANT P (Continued)
Storage
REQUIRED OR USED
BACK-UP SYSTEMS

Requires proper dike drain-
age system operation to in-
sure impounding of spills,
and the proper transfer to
waste disposal of the con-
tained spill

Manual gauging provides a
back-up for  the tanks with
continuously monitored
liquid level indicators
                                                 REMARKS

                                                 Dikes are required by fire
                                                 regulations
Storage
Operator must take
effective action
Storage
Appropriate  sewer  system
and waste water  treating
system  required
Only those leaks which occur
above ground can be handled
by this approach.
Processing,
transfer, others
Process,  other
                             Although such a system
                             maximizes the waste treatment
                             facilities necessary, it in-
                             sures  treatment of all liquids
                             leaving the plant facilities.
Regular  collection of waste
solvent,  acid,  etc.  and
transportation  to waste
disposal facilities  required
                                       163

-------
DESIGN CRITERIA. PROCEDURES AND EQUIPMENT IN OIL TERMINAL AND OIL REFINERY


              STORAGE AND DISTRIBUTION FACTLTTY - PLANT Q
                        ITEMS                                   TYPE

      1.  Each tank of any barge  operating  within  the            Equipment
         metropolitan district near  this  facility requires
         the use of a high-level alarm.
      2.   Standard  procedures  regularly used  to pressure        Procedure
          test  each flexible hose against a blind  flange
          bolted on the hose end.
      3. Flexible loading hoses preferred over swivel-         Equipment
         jointed, articulated loading arms.
      4. After a loading or unloading operation has been       Procedure
         completed at a marine terminal,  the hoses are
         drained by gravity either into the vessel or
         back into the shore-mounted storage tank (de-
         pending upon relative elevations).

      4. All storage tanks are equipped with level             Equipment
         indicators which register on a tank-side gauge.

      5. Manual tank gauging occurs regularly.                  Procedure
                                    164

-------
                          PLANT Q  (Continued)
                    REQUIRED OR USED
                    BACK-UP SYSTEMS
                    Appropriate action on  the
                    part of a  licensed tanker
                    man present on  the barge
                    during loading  operations
Loading
Loading
                             REMARKS

                             A high-level alarm in the
                             strict sense is not a fail-
                             safe device, and proper
                             functioning of such a device
                             tends to make operating per-
                             sonnel put absolute reliance
                             on the continued perfect
                             functioning of the equipment,
                             which in itself can be re-
                             sponsible for major spills in
                             the event of equipment failure

                             Leaks from flexible pressure
                             hoses due to damage incurred
                             during handling, or deterio-
                             ration resulting from their
                             normally exposed locations
                             dictates strict testing pro-
                             cedures .

                             Each swivel-joint viewed as a
                             point of vulnerability with
                             regard to leaks.  Experience
                             has shown that flexible hoses
                             give better, and more leak-fre
                             service than swivel-jointed ar
                             at marine terminals.
Loading and
unloading
Storage


Storage
Gauging of liquid levels
in all tanks by manual means,

Manual gauging provides
a backup  for  the  tanks
with continuously monitored
liquid level  indicators.
                                    165

-------
DESICH CRJ
                              rc EQUIPMENT    OIL TERMINAL AND OIL REFINERY.
             .STGR-jylT AX
                                 :-
                     ITEM
 6. A  single  sewer  treatment conveys all  rain-
   water  runoff and  any oil spills to  the
   waste  water treatment  system.
                                                          Design criteria
 7. All marine  terminals are equipped with an oil-
   water  separator.
                                                          Design criteria,
                                                          equipment
 8.  Practically all  piping  is  above  ground.
                                                          Design criteria
 9-  Regular periodic  inspection using standard  pro-       Procedure
    cedures for all piping  including hydrostatic
    testing and visual  inspection.

10.  Normal activities of plant operation requires         Procedure
    operators  to observe or  at least  walk along some
    of the exposed  pipelines during their daily
    activities.
 principal Hazardous Materials;  Oils, Hydrocarbons, Organic Products.
                                  166

-------
                        PLANT  Q (Continued)
AREA

Storage, others
REQUIRED OR USED
BACK-UP SYSTEMS
Storage, others
Waste water  treatment
system  following  oil-
water separator used
 Process,  other
 Transfer,  other
 Transfer,  other
REMARKS

Although this approach mini-
mizes the risk of untreated
spills leaving the facility
proper (if designed well) it
maximizes the size of waste
water treatment facilities
required.

An oil-water separator serves
the dual purpose of recovering
valuable petroleum products
which are spilled and carried
from the facilities with rain-
water or deluged flushing
systems required by various
insurance and fire codes, and
also serves to minimize the
treatment load placed on the
waste water treatment facili-
ties by a large spill of oil
or other petroleum products.

Permits immediate visual de-
tection of leaks or spills
associated with transfer pipe-
lines .

Primary purpose is to prevent
accidents—built-in spill pre-
vention and detection aspects.

Certain sample points or data
taking points are stratically
located in plant, such that
operators must regularly visit
these points--requiring their
visual observation of pipeline
and other equipment enroute.
                                     167

-------
                  ITEM

1.  Separate chemical sewer and clean water storm
   sewer drainage systems.
TYPE

Design criteria
2.  Practically all piping is above ground
Design criteria
3. Regular periodic inspection using standard pro-
   cedures for all piping,  including hydrostatic
   testing and visual inspection.
Procedure
4. Areas under transfer pipelines have concrete
   surface.

5. Suction trucks are used to remove waste chemicals
   collected in sumps during equipment "turn-around".
Design criteria
Procedure,
equipment
6. During loading or unloading operations between a
   tanker and the terminal,  the scupper plugs must
   be closed in order to contain any oil spill to
   the deck of the vessel.

7. Some storage tanks are equipped with high-level
   alarms.

&. Many storage tanks are surrounded by dikes.
Procedure
Design criteria,
equipment

Design criteria,
equipment
9. Manual tank gauging occurs regularly.

                               168
Procedure

-------
                            PLANT R (Continued)
AREA

Process, other



Process, other
Transfer,  other
Transfer,
processing

Processing,
other
Loading and
Unloading
REQUIRED OR USED
BACK-UP SYSTEMS
Grade, curbing, and
drainage system required.

Regular chemical sewer
system and waste treat-
ment facilities used.
Means for removing oil-
contained on deck required.
                             REMARKS

                             Insures chemical spills do
                             not get into the rainwater
                             discharge from the facilities

                             Permits immediate visual de-
                             tection of leaks or spills
                             associated with transfer pipe-
                             lines.

                             Primary purpose is to prevent
                             accidents—built-in spill
                             prevention and detection
                             aspects.
                             Waste materials from equip-
                             ment cleaning operations are
                             removed in a concentrated
                             form, thereby facilitating
                             disposal.
Storage


Storage
Storage
Operator required to
take effective action

Requires proper dike drain-
age system operation to in-
sure impounding of spills,
and the proper, transfer to
waste disposal of the con-
tained spill.

Manual gauging provides a
backup for the tanks with
continuously monitored
liquid level indicators.
                             Dikes are required by fire
                             regulations, but also serve
                             as an effective "fail-safe"
                             spill prevention measure.
                                  169

-------
                    PLANT R (Continued)
             ITEMS

10.  Computer control capability for monitoring
    and controlling all of the liquid moves
    associated with the storage tanks  terminals,
    and pipelines.
TYPE

Design criteria
11. The sludge which is removed from the bottom
    rf storage tanks during their periodic cleaning
    is performed on a contract basis and is removed
    by the waste disposal contractor.

12. Samples of waste water moving through the sewer
    systems and the waste disposal facilities are
    regularly monitored for pH, Toe, and oil
    content.

13. All surge  tanks are located at the offsites
    with the final product storage tanks.
Procedure
Procedure
Design criteria
14. Standard procedures established for communi-
    cating between ship and shore during loading
    and unloading operations at the marine terminal
Procedure
Principal Hazardous Materials-   Oils,  Hydrocarbons, Organic Products.

                                170

-------
                             PLANT R (Continued)
AREA

Storage,
other
REQUIRED OR USED
BACK-UP SYSTEMS
 Storage
 Process,
 Other
 Diversion or  other
 facilities  to hold
 fluids outside normal
 tolerances  required
                             REMARKS

                             This  system  is  presently  in
                             the early  stages of evolution,
                             but the  intent  is clearly to
                             provide  a  computerized system
                             to handle  the logistics of the
                             movement and storage of liquid
                             in a  complex refinery/terminal
                             operation, from which close
                             inventory  control and leak
                             detection  should be resulting
                             by-products.

                             Industry appears to be turning
                             to this  solution for the  dis-
                             posal of materials which  are
                             difficult  to treat.
 Storage,
 Other
 Loading and
 unloading
                                    171
                             Any'over  filling of surge
                             tanks due  to problems or error?
                             in operation in the processing
                             areas will result  in spills
                             which can  contained and handle
                             by the  facilities  which exist
                             for  this  purpose at the storag
                             areas.

                             Communications between ship an.
                             shore during unloading of  largv
                             oceangoing tankers at marine
                             terminals  can be a significant
                             problem with the relatively
                             small crews extant on todays
                             large supertankers, and the
                             language  barriers  which often
                             exist when large tankers are
                             manned  by non-English speaking
                             crews.

-------
DESIGN CRITERIA. PROCEDURES AND EQUIPMENT IN CHEMICAL  FACILITY - PLANT S
                      ITEMS                               TYPE


1. Only storage tanks  containing flammable liquids       Design criteria,
   are surrounded by dikes.                               equipment
2. A single sewer handles  all  rainwater  and chemical     Design criteria
   spills.
3. A holding and  neutralization  pond  is  used  to in-      Design criteria,
   crease pH to approximately 6  -  7 by the  use of        procedure
   lime additions to neutralize  normally acidic
   chemical waste materials.
4. Process areas  built on proper  grade  to direct  any     Design criteria
   spills to sewer system.
5. Process areas  and other  areas  where  strong acids       Design criteria
   are used are surrounded  b y  curbing  to direct
   the flow of any spilled  liquids  to the sewer
   system.

6. Process areas  handling the most  hazardous  materials   Design criteria,
   from a pollution viewpoint are completely  sur-        equipment
   rounded by dikes  drainage ditches,  etc. and are
   provided with  specific waste treatment facilities
   designed specifically for those  materials  being
   handled.
Principal Hazardous Materials;  Acids, Inorganics.
                                 172

-------
                       P1.ANT S (Continued)
                    REQUIRED OR USED
                    BACK-UP SYSTEMS              REMARKS
Process,
others
Process,
other
Process
Process,
other
Requires proper dike
drainage system opera-
tion to insure impounding
of spills, and the proper
transfer of waste dis-
posal of the contained
spill

Appropriate impounding
and waste disposal treat-
ment facilities required
Continuous pH measurement
by submerged electrodes,
with periodic check and
calibration of instrumen-
tation by plant personnel used

Adequate sewer system to
Convey  spills to waste
treatment facilities required

Appropriate sewer system
to convey spills to waste
treatment facilities  required
                                                 Dikes are required by fire
                                                 regulations, but also serve
                                                 as an effective "fail-safe"
                                                 spill prevention measure.
Process
The main waste  treatment
facilities  of the  plant
provide backup  for  the
specialized waste  treat-
ment  facilities  serving
the hazardous process area
                                 173

-------
DESIGN CRITERIA. PROCEDURES AND EQUIPMENT IN CHEMICAL  FACII-TTV - PLANT T
                ITEMS                                     TYPE

  1. All of the processing units are located on concrete   Design  criteria
    surface areas.

  2. All concrete surface areas under processing           Design  criteria
    units are constructed with a sloping grade
    toward drainage ditches.
  3. Concrete  lined ditches surround the concrete          Design  criteria
    surfaced  areas on which all processing units
    are  located.                                                 :

  4. All piping above ground on overhead                   Design  criteria
    pipe racks.
  5. The  plant affluent stream is continuously             Design  criteria,
    monitored for BOD and TOD.                            equipment
  6. The activated sludge plant is equipped with           Design  criteria,
    a  continuous TOD analyzer and recorder and            equipment
    alarm system.

  7. The first one-half inch of rainfall goes              Design  criteria
    through the neutralizing and treating
    ponds, while the remainder of each rain-
    fall is discharged directly into the nearby
    watercourse.
  8. Flexible  loading hoses are blown clean with            "Procedure
    nitrogen  into the vessel being  loaded after
    the  filling operation has been  completed.
                                   174

-------
                            PLANT T (Continued)
                    REQUIRED OR USED
                    BACK-UP SYSTEMS
Process
process
Appropriate sewer system
to remove spills required.
                             REMARKS

                             Prevents penetration of any
                             spilled liquids into the soil.

                             Spills are controlled by being
                             directed away from their
                             source toward the disposal
                             facilities provided.
          transfer
Waste  treatment,
other
Waste  treatment
 Process,  other
This is a backup
system for  the
main waste  treat-
ment facilities.

This is a backup system
for the main waste
treatment facilities.
Loading and
unloading
                             Permits visual detec-
                             tion of leaks or spills
                             associated with transfer
                             pipelines.
                             The potentially dirty
                             initial rainwater run-
                             off is treated, while
                             the typically clean
                             rainwater runoff from
                             the latter part of each
                             storm is diverted directly
                             into the watercourse.

                             This  procedure minimizes
                             the  liquid to  be  drained  and
                             collected  from the  loading
                             hose  after each loading opera-
                             tion  has  been  completed.
                                   175

-------
DESIGN CRITERIA.'  PROCEDURES AND EQUIPMENT IN CHEMICAL FACILITY - PUNT T (Continued)
                     ITEMS

      9. When not used, loading hoses are capped to prevent
         drips.

     10. Tank cars and trucks are filled entirely by manual
         operations.

     11. The product tanks from which liquids are moved to
         the terminal location are mounted on load-cells
         which continuously weigh  the total tank plus
         contents.
TYPE

Procedure


Procedure
Design criteria,
equipment
     12. Specific storage tanks are surrounded by con-
         crete fire walls (dikes)
Design criteria
     Principal Hazardous Materials;  Isocyanates, Amimes Caustic, Inorganic Acids.
                                       176

-------
                          .   PLANT T (Continued)
AREA

Loading and
unloading

Loading and
unloading

Storage,
 loading and
 unloading
REQUIRED OR USED
BACK-UP SYSTEMS
Requires continuous
operator attention

Data transmission
and operator  action
required
REMARKS
 Storage
Appropriate  fire wall
drainage and sewer
systems required.
This provides a direct and
continuous monitoring of the
total liquids moved from the
storage tanks to the rail
cars or tank trucks. It is don
primarily for safety reasons,
and because of the very high
value of the products moved at
this plant.  However, this
system also provides a means
for quickly determining spills
of liquids associated with
the storage facilities.

Dikes surround only the tanks
containing flammable liquids.
as dictated by fire regulation
however, these dikes also serv
as an effective "fail-safe"
spill prevention measure.
                                      177

-------
DESIGN CRITERIA
                 PROCEDURES AND EQUIPMENT IN THE PETROCHEMICAL, CHEMICAL AND PLASTICS   FACILITY -
                                       PLANT U
                         ITEMS
                                                                   TYPE
          1. Most of the production  units  are  located  on concrete  Design criteria
             pads.
          2. Concrete pad areas are built on a grade to direct
             chemical spills.

          3. Curbing and/or ditches surround process unit
             concrete pad areas.

          4. Many production units are equipped with a
             separate chemical sewer system-
Design criteria


Design criteria


Design criteria
          5. All other process concrete pad areas are serviced     Design criteria
             by a single sewer system.
          6. Certain production units are equipped with unit
             oil separators and/or other waste treatment
             facilities.
Design criteria,
equipment
          7. All of the loading and unloading terminal fa-
             cilities which service carriers other than
             barges or vessels are built over concrete
             surfaced areas.
                      /

          8. Concrete surfaced loading and unloading areas are
             graded toward drains connecting with the general
             sewer system.
Design criteria
Design criteria
                                              178

-------
                              PLANT U (Continued)
Process
Process
                    REQUIRED OR USED
                    BACK-UP SYSTEMS
                             REMARKS
Suitable means for directing Insures that chemical spills
spills of liquids to col-    are simply not absorbed into
lection and disposal         the soil.
facilities required

Suitable collection and
handling means required

Suitable sewer system
required
Process
Process
Process
Suitable waste disposal
facilities required
A suitable single waste
water  treatment  facility
required
Main waste  treatment
facilities  required
This is provided for the
production units which handle
or produce water soluble
organic materials.

Processing areas which produce
organic chemical liquids
which are not soluble  in
water are serviced  by  the same
sewer system which  handles
rainwater runnoff.

This not only reduces  the
total load on the central
waste treatment facilities
serving this plant, but also
permit more specific tailoring
of the kind of waste treatment
facilities used for each new
unit.
Loading  and
unloading
 Suitable sewer
 system  required
Loading and
unloading
Suitable waste disposal
facilities  required
                                    179

-------
DESIGN CRITERIA. PROCEDURES AND EQUIPMENT IN THE PETROCHEMICAL. CHEMICAL AND PLASTIC^  FACILITY -


                                   PLANT U  (Continued)



                           ITEMS                                      TYPE

             9. Rail car and tank truck washing facilities are        Design criteria
                built on concrete surfaced areas which are con-
                nected to a unit oil separator and then to the
                sewer system.

            10. The first one-half inch to one inch of rainfall       Design criteria
                over the entire plant area which is served by
                storm sewers drains into and is held by a large
                holding lagoon.
            11. Suction trucks are used to remove waste sludge        Procedure,
                from the bottom of storage tanks.                     equipment
            12. Vacuum trucks are used for removing large spills       Procedure,
                which are confined in specific areas such as          equipment
                behind dikes or curbing.

            13. A continuous TOD monitoring system is being           Equipment.
                developed.                                            design criteria

            14. Gas chromotography is being used to identify          Procedure
                specific organic compounds contained in the
                waste water system.
                                             180

-------
                              Plant U Continued)
AREA

Loading and
unloading
REQUIRED OR USED
BACK-UP SYSTEMS

Suitable waste  disposal
facilities required.
REMARKS
Waste  treatment
 Storage
 Storage,  other
This is a backup
system for  the
main waste  treat-
ment facilities to  even
out the load  imposed on
it by rainstorms.
                                                  After the first one-half inch
                                                  to one inch of rainfall, it has-
                                                  been found that the entire plant
                                                  area will have been cleaned of
                                                  chemical and oil spills.  After
                                                  this quantity of rainfall has
                                                  run off and has been collected
                                                  by the large storage lagoon,
                                                  the remainder of the rainfall
                                                  is discharged directly to the
                                                  watercourse  since it is es-
                                                  sentially clean.  After the
                                                  rain has stopped, the oily
                                                  water stored in the large
                                                  lagoon can be slowly fed into
                                                  the water treatment system.
 The  remainder of the sludge
 is washed from the -bottom
 of the tank with water and
 drained to the sewer system.

 Specific waste disposal
 facilities required.
The use of vacuum trucks for
such purposes is increasing.
 Process,  waste
 treatment,  others

 Waste treatment,
 others.
 This is a backup
 system for processing
 operations.
The presence of any organic
products in excess of the
acceptable limits set by the
company is traced to the speci-
fic operator responsible.  This
is perhaps the essence of spill
prevention.
                                     181

-------
DESIGN CRITERIA.  PROCEDURES AND EQUIPMENT  IN  THE  PETROCHEMICAL.  CHEMICAL ANn PTA
-------
                              PLANT U  (Continued)
                    REQUIRED OR USED
AREA                BACK-UP SYSTEMS               REMARKS

Process,            Appropriate operator         This decreases the lag time
other               action,required.              between a spill of specific
                                                  products, reactants,  or inter-
                                                  mediates at their source,  and
                                                  the detection of these chemica
                                                  This approach to spill detec-
                                                  tion is highly favored, and
                                                  is'.Increasing in its  use.
                                     183

-------
DESIGN CRITERIA, PROCEDURES  AND  EQUIPMENT IN   CHEMICAL AND PETROCHEMICAL   FACILITY -  PLANT V
                          ITEMS

             1. All of the process units are built on concrete
                pads .
                                                                      TYPE
Design criteria
             2. All storage tanks are diked.

             3  The first inch of rain which  runs off the
                entire plant area goes to a storm water holding
                pond.
Design criteria

Design criteria
                Separate chemical sewer and clean water storm
                sewer drainage systems.
Design criteria
             6. A separate chemical sewer takes spills from
                specially curbed areas such as around pumps and
                certain process units which produce either a
                continuous discharge or have a high risk of
                chemical spills.

             7. All storage tanks are surrounded by dikes.
Design criteria
Design criteria
             8. The rail car loading area is graded to drain to
                a concrete lined trough paralleling the rail
                tracks and located on each side of the tracks.

             9  The troughs which handle spills at the rail car
                loading and unloading facilities empty into a
                special catchment basin with a capacity equiva-
                lent to one inch of rainfall on the entire track
                loading terminal area
Design criteria
Design criteria
                                              184

-------
                               PLANT V (Continued)
Storage, other

Process, other
Process, other
Process,  other
                    REQUIRED  OR USED
                    BACK-UP SYSTEM
                                                 REMARKS
                    Suitable means  for  col-
                    lecting and  treating
                    waste chemical  spills.required.
Suitable waste treatment
facilities required.
Suitable waste disposal
facilities used.
After the first inch of rain
runs off the plant area,  it
is clean, thereby permitting
the remaining rainwater to
run off directly to the nearby
watercourse.

Insures chemical spills do  not
get into the rainwater dis-
charge from the facilities.
Storage,  other
 loading  and
 unloading
T    i-;s proper
diainage system  operation
to  insure  Impounding of
spills, and  the  proper
transfer to  waste disposal
of  the  contained spill.

Suitable sewer system  to
handle  spills required.
Dikes are required by fire
regulations, but also serve as
an effective "fail-safe" spill
prevention measure.
Loading and
unloading
Suitable waste  disposal
facilities required.
                                     185

-------
      DESIGN CRITERIA. PROCEDURES AND EQUIPMENT IN CHEMICAL AND PETROCHEMICAL FACILITY

                                   PLANT V  (Continued)
                  ITEMS                                   TYPE                  AREA

10.  The  entire  marine  terminal dock  is constructed        Design  criteria       Loading and
    of concrete,  is  curbed,  and has  its  surface                                 unloading
    slrped  toward  stainless  steel drains.

11   At the  conclusion  of  loading operations, the on-      Design  criteria,      Loading and
    shore valve is closed, and the hose  between the       procedure             unloading
    valve and  the  barge is blown out using pressurized
    nitrogen.

12.  Remote  shutdown  for loading transfer pumps.           Design  criteria.      Loading and
                                                         equipment             unloading
Principal Hazardous Materials;   Ethylene,  Acetic  Acid,  Cyclohexane,  Organlcs.
                                         186

-------
              PLANT V  (Continued)
REQUIRED OR USED
BACK-UP SYSTEM               REMARKS

Stainless steel waste
storage tank located
below dock area used.
This is a backup             This remote control for the
system for the               loading  pump  is a safety re-
directly controlled          quirement, but also functions
loading operation under      as  an environmental protection
the supervision of a  ,       feature.
registered tanker man.
                        187

-------
DFSIGN CRITERIA, PROCEDURES AND EQUIPMENT IN CHEMICAL  FACILITY  -  PLANT W
                   ITEMS                          "         TYPE

   1. Some storage tanks are diked.                          Design criteria
   2. Regular periodic inspection using standard            Procedure
      procedures for all piping including hydro-
      static testing and visual inspection.
    Principal Hazardous Materials;   Inorganic Solids
                                 188

-------
                       PLANT W  (Continued)
                    REQUIRED  OR USED
AREA                BACK-UP SYSTEMS               REMARKS

Storage             Suitable  means for trans-    Dikes are required by fire
                    porting and handling waste   regulations,  and therefore
                    chemical  spills required.    surround tanks containing
                                                  flammable materials only;
                                                  dikes however also serve as
                                                  an effective "fail-safe" spill
                                                  prevention measure.

Transfer,  other                                  Primary purpose is to prevent
                                                  accidents--built-in spill
                                                  prevention and detection as-
                                                  pects.
                                    189

-------
DESIGN CRITERIA.  EQUIPMENT AND PROCEDURES USED BY ARCHITECT-ENGINEERING FIRMS
               ITEM                  TYPE        AREA

  1.  Location by area function,     Design        all
     i.e., process, storage,       Criteria
     loading  utility, etc.

  2.  Dual Sewers in loading &       Design     Loading &
     unloading area, one for       Criteria    Unloading
     spills, one for rain runoff

  3.  Hard surfacing of loading      Design     Loading &
     and unloading area            Criteria    Unloading
                           BACK-UP SYSTEMS
                           not applicable
                           Curbed area &
                           hard surfacing
                           Curbs and
                           separate sewers
     Curbing
        (a) Process
        (b) Loading
        (c) Unloading
        (d) Transfer

     Gravel or shell covering
     of  loading
Design
Criteria
 Design
Criteria
Process
Loading
Unloading
Transfer

Loading &
Unloading
                          Sloping surface
                          to appropriate
                          sewer
Grade to sewer
     Flame Arresters in
     Sewer Systems

     Loading arms and "dead
     man" controls
  8.  Drip pans under selected
     joints, etc., in loading
     and unloading area

  9.  Dikes around storage tanks
        (a) Flammable Liquids
        (b) Non-Flammable Liquids

  10.  Process Wastewater
      Treatment Plant
 Design
Criteria

 Design
Criteria,
Equipment
   all
Loading
 Design     Loading &
 Criteria   Unloading
 Equipment
 Design
Criteria,
 Design
Criteria,
 Storage
   all
Hard surfaced,
sewered areas
              Plant Collection
              system
Fail-safe valve
system in diked
area for drainage

Catchment basins
or holding  lagoons
  11.  Holding Lagoon
 Design
Criteria
   all
Diversionary Sewers,
etc.
                                     190

-------
DESIGN CRITERIA, EQUIPMENT AND  PROCEDURES  USED BY ARCHITECT-ENGINEERING FIRMS

                             (Continued)
             Company Recommended or Industry Standard  If Required by Client
         REMARKS        /            Companies              Companies
                                AA  AB  AC  AD  AJE      AA  AB  AC  AD  AE
 Systematizes Designs and       X   X   X   X   X
 Spill Control Problem
 Permits special handling
 of most hazardous concen-
 trations

 Permits special handling
 of most hazardous concen-
 trations
X   X   X   X
X   X   X   X
 Controlling spread of liquids  X   X
       11        "         "XX
 Essentially for personnel
 convenience.  Requires all
 rainwater treatment

 To prevent spread of flames
 via sewer system

 Reduce dependency on
 operator attention
                                X
                                X
    X
    X
X
X
X
X
X
X
X
X
X
X
X
X
X   X   X   X   X
        X
                                  X   X
 Low cost,  selective
 control  system
                                                       X   X   X   X   X
  Passive Barrier,
  Primary Defense
                                X   X   X   X   X
                       X   X   X   X   X
  Permits  removal  of  spilled
  materials  on  controlled
  basis

  Permits  segregation for  con-
  trolled  treatment or release
X   X   X   X   X
XXX
                                      191

-------
DESIGN CRITERIA, EQUIPMENT AND PROCEDURES USED BY ARCHITECT-ENGINEERING FIRMS  (continued^
                  ITEM
   TYPE
                                                    AREA
                            BACK-UP SYSTEMS
     12.   Selective Segregation
          of Storm Water
  Design
 Criteria,
Procedure
                                                     all
              Diversinary
              mechanism
     13.   Separate Process  sewers
          from  process area drainage
  Design      Process       Wastewater Treat-
 Criteria,                  ment plant &
Procedure                   holding lagoon
     14.  High&low  liquid  level alarms
         on  storage &  process tanks

     15.  Above  ground  piping on
         racks
 Design
 Criteria
 Design
 Criteria
Process &
Storage

Process
Transfer
Monitors and
alarms

Drainage collec-
tion under rack
     16.  Fixed  Boom  loading arms  in-   Design       Transfer
         stead  of hoses on marine
         facilities
     17.   Tank  Hydrostatic Testing     Procedure    Storage,
          Program                                   Process
     18.   Manual  Pump  out  connections
          for  tank  emptying
 Design
 Criteria,
 Procedure
Storage
                            Curbed areas
Spare Tankage
     19.  Automatic Controls on pH at
         wastewater  treatment plant
     20.  Liquid  knockout drums on
         gas  relief system
     21.   Installation of fin-
          fan  coolers

     22. Detection Instrumentation in
        wastewater  lines-especially
        oil

     23.   All  welded  transfer piping
          systems
  Design
 Criteria,
 Equipment

   Design
  Criteria,
 Equipment
   Design,
   Criteria
   Design,
   Criteria
   Equipment
    Design
    Criteria
Waste
Treatment


Process



Process


Process
Process
Transfer
Process Drainage
                                          192

-------
DESIGN CRITERIA, EQUIPMENT AND PROCEDURES USED BY ARCHITECT-ENGINEERING FIRMS

                                     (Continued)
                 Company Recommended or Industry Standard If Required by Client
            REMARKS                     Companies                Companies
                                   AAAIBACADAE      £A  £B  £C  ££  M.
    Permits  holdup of initial      X   X   X   X                           X
    storm runoff for subsequent
    treatment
    Permits most effective
    treatments
X   X
    X
    Active detection
                                                              X
    Prevents uncontrolled spread   X
    of liquids from pipe breaks

    Pipelines should be periodi-
    cally tested

    Recommendation to client—no
    responsibility for program

    Removal to permit repairs
    X
X
                    X   X
                X   X
            X  X
    Rapid response to control
X
X   X
    Prevents liquids from being
    blown onto uncontrolled areas
    Replace water cooling  system
                                                           X   X
    Active alarm
                                                           XXX
                               X
    Reduces potential of  leaks     X '  X   XX    X
    from flanges
                                        193

-------
                  APPENDIX G

       TYPICAL PROCEDURE (JOB STANDARD)
  FOR TRANSFER OPERATION IN CHEMICAL INDUSTRY

        TYPICAL OPERATING STANDARD AND
CHECK LIST FOR LOADING AND DISCHARGING OF SHIPS
                        195

-------
                                         JOB STANDARD
                        JUtS oiAINUAKU

 37"::\  rz-:i SCALE TAT; TO •.*. FIF.U STO.V.G:,  V^T nc:

.::, VALV.-.S, F-'T, AH 5/312!,  FLO..' ir.UM,  J.U, TAG

Li:rr r:ivi5io:>
                                                                                          Ptant  Svtt. No Rf
                                                                                         L 4>;> ra 15^;
UX-AT1CN
MACHIt.
IOUIPW
TOOL*
                                                                       FIELD & CLD3. J25
 MACHINE .~J
 IOUIPWENT OAT*
 PA.'.t  .  OF  -

 SUPERSEDES    ACE

	PdLJJWB_	
Nt \S( )v. I OK
W ' H5I liLHL
                                                                                             fAJlTICIPANTS

                                                                                                   1
                                                                                             No,
      .1 U M 0
    CHART
                                    WORK FRODUCHD SHOULD BE VERIFIED BY
             REPORT
             Foto No.
                                          ACTUAL
                                        OBSERVATION
                                                                                             Opi-r.ition Studied
             No.
                   NORMAL FREUUtNCY
                    T (' _ ' t'_^_ ;
                            ELEMEKTS IN FULL DETAIL
                     Wot* EUmcnl, MUM B. PctfonntJ A. Dcxribcd Wo*
                                                                             REF FILE No
                                                                                           Occ P«
                   \.   JrO P STOCK r^OM 3C.\1.?. T.^K i?120 TO U'L'-T FIL1D T.V«C  V.ILN :
                       sv^L"  is :;I:.O;-.D  (Els. 1-7, 9,  11-13, 13,  13, 20-22)
                    .   A;;ITIC-:\L ALLO:A:;CL ro:i TA'a;;a FLO..' n.u*:t s-Vi-LC  ra:
                       Ar?:io:a."Axri.Y 9/10  rr:?i:;o3 (1:1-.. 3, 10, 1-'*, l'->. 17, 19)
                   c.   TJ-TAL ALLCr.'.'.rrc TO  rivj? 37oc:; r?.a:t ;;C,VLE  TA:H; tn20
                       FILLT r\-::: '..ir:i FLOT-; rrc*t S.VTLE i^ m;visno (Us.
                                                                                         3a-"3ple
                    ...-.Ik  to"ocalo Cai^ (if* av;;.)(.0012).   Set scalca  aaJ check
                    vci-'r.t  of stock  in t.mk (.0014).  Hecoril In pocl:ct notcboo!;
                    (.0024).

                   :.*r. Ain_o:!.U'^;
                   .ir.o  is not uicli air to be aura that line ia set to  carrcct  t.nk
                       ilk to air vilvc;i £i\)iip at
    > ij.ib u^ »»i i.  v i^vw;^ ^..w.^/  .jh. i..-....*  \3^  tiV^. } \»'-"-"_ .I/ .  C»3^Q UXO
    naJ open t-.-o  3/V v.ilvc-.;  to ti;m  0:1 air (.0042).  Return to fr
    of  scxilo t;j;ii (33' avj.)(.C024).                           ,

  ij-C---^./'••: .^-*, •'.-'• •^*,     '      -•     •  ""     <   • 5t-i'-,-  ^; j^«..-:
    lull cl: :ia cutc-iuiana to  open ono 2!y v.ilve nnj close ono 2%"
    vilvo a'jovc n.iin aisle  (.0030).   Go to area acir pi^-?, pull
    c'.:.iln e:;tc;isVo-.i3 to open  one 2'."'  vjlvo o:iJ clo^o 2V v:ilvo
    (.0033).  CD  to ?:6 tci:s.->aina level (53' av-.  * 21 su)(.0037).
    Check 2 - 3'1  v.-jlvas on:! open or close or.o 3''  valvo (.0353).
    Step to £. slUe of ^es.-:.5nlno (5').   Chen!: r-n  av^. of ono 4"
    viive.  Open  or clo-o 3 - 4" v.lvos (.0104).   Walk to arc.wny
    south of s:=3  bsut. (00* * 21 s-J + 4 5u)(.00')7).  Open o.n4 clos(
    an  QV3. of 4  -  4" valves  to set lino (.0165).

  :I:T LT:njTOFi.M.o TA::^.	c;.".:c:c AI:I  Ti;tr/;.";i
                                                                                         -Jcr
                                                                                         nt
                     W:\lk frou vnlvc.T near S'^i bjst..:crit cjor  to vnlvo groi») at end
                     (vent) of nrcaway by storeroom (216') (.0126).  Open one 4" v.il'
                     Close ono 4" v.ilvo  (.0110).   W-.l'.; to valvo group outside west
                     j**tp house (193* +  14 su).  Observe 3 valves  on line to be sure
                     tfa«y are  s«t properly (.0144).  Open one 4" valve, close  2-4"
                     valves (.0165).  Step to weet  tank Cant (57* + 3 su).  Open and
                     closo an  ovs. of 3  valves to  set  lino to tank.  Walk on. av«.
                     of 154' + 2 sd while setting  lino (.0775).  Clor.o tone 4" vnlvc
                     on line.   Open rls«r valve on tank slowly  to feel rush of air
                     Into tank (.0072).
                                                                                                  STD HRS.
                                                                               J .5732

                                                                                 .0522
                                                                                                   .0050
                                                                                                   .COJO
                                                                                                   .0745
                                                                                                    1302
                 l/yr. ai
                                   STUDIED BY   S.7
                                   CHANCES BY
                                                                TOTALSTO. HRS PER CCO SU^TUJtV
IT. » O-ERJC .
l-P!«nl
) L F- Div. .

4. D^L Mgr. .
I. Croup Mgr
                                 D«Pt Mgr.
                                                              GroiTpMgr
                 EfTEC
                                               196
                                                                Ind. Enn.
                                                              pUnt M
                                                                        Dt
                                                                             Audi""
                                                                                   "

                                                                                          D«
                                                                                               Auditor
                                                                                                     M.
                                                                                                       1.1

-------
r
*
. -OO'-'CT tnj
LOCATION
                      JOB STANDARD
                                                                        L /.OO Pd
PUT STOCK F7.0?! SCALE TX. TO  ',.'.  FILLD
                                          T, W. flLL) 4 25U>G« £26
             No.
            10
            li
            12
            13
            14
                 :l
                                                   IN FULL DETAIL
                                                                8 is obtalncjd.
                     Open \" valvo  In line to flov droa (.0014).  i^lk to flow dru
                     (151 avj.).  Step up to flow druz3.   Inspect anJ adjust flow lnt>
                     flo:v druni.  Step clav.'n fro.-j drta (.0-^9).
                               _
                     Walk to storage tank i» W. tank farm to which oil is being
                     puaped (688' + 21 a« + 2 sd -»• od)(.C427).  Note  flow of oil
                     Into tank by placing car againat riser pipe line (.0010).
                     Return to S&S  b«rt.  (674' + 21 au + 2 su + od)(.0468)
                     V.'::i,n at o.KC.ifor's Uo-'.:, G-'-^ -<-V-:plc  t:'-J  fro.i --raver in dc^U
                     Till la ace.  infoivution on s.;::pic t^ (.CD70).   Get e-v^lc
                        k frou Jc.'--;  an-1 pencil £I-D:- po;l:ct.   fill out tho ncceaj
                             iori in  tlie 3a;,plo 'jo:/.; relativo  to na.,  co^'c, stack,
                     etc. (.OOS3).   '..'aIk frs i other v;ork  l;j area  ta cxjplo jr.r atora
                     at t.jn'c 110 (j1).  Get  liner, place  liner in cap an«l s_ro"?.t:r=t>  o?
                                                           (.0029)
                     Uaii: iron other vorU to acala (10' ovj.).  Balance scalo for
                     opprox. wc-l^ht  to noto prosross o; pulping (40,000^ avs. pvc--plnk).
ATT;:: mo:: TO LAST o?_yi? ffUjc
  Walk rro.3*othor worU  to scale  (10'  nv
                                                                 Watch anJ soove scale
                     boa.-a v'lllo pippins -last of stock frt^ scale tan!«,
       "to rear oi Vealo"tank  (35'  av3.)(.0025).  Close vaivo  in
  lino unJ«r tanU (.0355).  Open two 1;' valves, close bleeder to
  air  blov lino fros scale tanU to vest fara tank (.0033).

     o:: .'.GIT.MC:I i:? FT.O.J. orx:i
     'iTTlo^ (jrua ~ust ajltato for  at lea-st 2-3 alnutoj before
takln-r oacsplo.  Tills i« done  to l:uuro well nintd sa^?lo.
  Jtep to aov drua (12' + 2  su r.vj.).  Open I" valve to turn on
  nir  to  contents of flow drua (.0029).
2  OF 3
                                                                            STO HRS


                                                                            .0063
                                                                                              .0118
                                                                                             .0305
                                                                           .01GC
                                                                                .0115
                                                                                             .0300
                                                                                             .0133
                                                                                             .0025
              COPT:  1. T.B. CLERI
                                   2. PL»»T I.C.
                                                    3. I.S. DIV.
                                                                          Bgr.
                                                                                    . Group Mgr.

-------
  «-•<»       I
_L
                            JOB  STANDARD
                                                                      L 600 Pd  1T-'.C   pu"' **
                                                                    LX.6 ELDG«  ?2j
    q
     t
15
             16
;MtN'1S IrJ fV'l-L DETAIL
i .v u»i P^ P.-T 111 i-.*\J A * CV*rTib"«J Mow
             17
             20
             21
             22
                                 .
                     V.ilk to  pu p cvltch (1G* avj.), p-:sb button to stop pmp(.C020)j.
                     Ualk to  ot'.K-r worl: (30'),  vMlo flo^ CHJ.I njltctcs (.0022).
                     ..'alii to  sc.ilo"ta;'_: (11'),  2C^ s^..:?le bcttle, valk to  flov Urur.
                     (25' -»• 2 cu)(.C035).  "c_ow c^p on:', place In pocl;c-t»  u>o Ulppdr
                     t^ Clp ca--plc fr:/n flow  drvc to t^plo Lottie or jar»  cap bottlp
                     (.O062).  C1030 V:" valvo to turn off olr  (.0014).
                            .
                      .-.tn 2!1  wotto.a v;-.vo to
                                       cJr.2.; (.0023).  Valk (4» nv~.), pus
                             starting j>uv.p  (.0012).  ?.ctum en*;1, c'.icci p-^.pln^ fro'.i
                     fl-j Ci-uu! (.01CO).  Step uavn anJ close  2" bottom valx-c of
                     flow tlruu (.003-4).

                    :;;;^C ;ri , AI ^_T o J'I/A:^ to?) ^.^y 71 J:_LT: u:
                     w'^li: to ,:ir valv:.-j (20*  avj,.), clo.oo bleeder and open two valve
                     to tura on air to blo-j lino (.0333).  Walk to T»V.-»>  (341
                                                                                          PAI .E
                                                                                  3  °F3
                                                                                         Occ. Per
                     set c.nplc (1C r-:iy) csiCo on sc.-le of t.^i'- (.OJ26).   Open blccc
                     clicclc air tl:rou^li pu.-.,?,  cloao blco^cr (.OC3i).
                     l'u-li  li.ct'Ki to £1:^.-:) p?j .p (.CCC6).  O-ion  I," flo-j l!no valve.
                     Cloio 2-V' valve in lir.o froa i>'-'c I? co *'S tc> force air tl;r»ush
                     s.^rplc lino ta flov Oru:i.  Dlow line.  Open 2';" valve.   Close
                     I" v.ilvc (.0073).
                    l,ic  to W.  field -.:Li.at be  blov.i Cor at  Ic :ct 20 uiivj^cs  to clear
                     lino.
                     'il-ill:  to air v.ilvcj (30*  aV2.)(.0022).   Cloijc 2 air valve .5, open
                     blccJcr (.0^2).
                     ».ii: tu  .rJ; ia vr.;c   icl.J (603' * 21  GII *• 2 a I * oj){.0*>17).
                     C-.u^o tuiLC onj record  In jvnli (.0030).   Clouo f»" riccr v;:lvo on
                     tarl; (.COjS)-  Ilcturii  Co ccjlc tanl:  In brr.at. (603' +  21 sd + 2
                     Sut  ccr.lca ,i:ij c:-.cct:  flail wclclst  (.CC42).  Subtract  Cinnl uei;
                     froj st-u-Clnj uc..-:.t  Co calculalre  not uoljht pu'.r^cd  (.0340).
                     ::.-.i:o r.ecccsary cn'cric-3  on pujp ol.cot.   Show tanl: noa.,  a'jount
                     pu-rpcJ,  etc. C.CC33).
                   5/1C/GG bS
                                             198
               COPT:  1. T.B. CITRI
                                                     3.  I.S.  DIV.
                                                                                                .0111
                                                                                                .0174
                                                                                    .0113
                                                                                                .0079
                                                                                   .OCS4
                                                                                                .C925
                                                                                                .0175
                                                                     4. D»pt. »gr.
                                                                                     5. Croup »gr.

-------
                                                  STANDARD OIL COMPANY OF CALIFORNIA
                                                  WESTERN OPERATIONS,  INC.
                                                  RICHMOND,  CALIFORNIA
VESSEL'S NAME
Our Operating Standard RE-3110 "Loading  and  Discharging Ships  at  Manufacturing Department
Terminals" describes the rules and  regulation  governing the operation  of  this Wharf.  A
complete copy la available  for you  to  read upon request. The  following is an abstract of
these rules and regulations:

   I.  "Class A" products include all  oils under 115*? closed  cup flash or all oils handled
       at or above their closed  cup flash  temperature  or all oils loaded into a tank con-
       tainir? Class A products  and not  subsequently gas freed.
   2.  "Claps B" products include all  oils of 115*P and higher closed cup  flash when
       handled at temperatures below their flash temperature.
   3.  No smoking on the Wharf or in the Berth  Offices.
   4.  No smoking on the weather decks of  your  Ship.   Smoking  peroitted aboard ship only in
       locations designated by the  Master.  Portholes  on the Wharf aide shall be kept
       closed or screened while  ship IB  along side Wharf.   Doors  and portholes facing load-
       ing decks shall be kept closed  except for momentary  passage.
   5.  In case of fire, stop  cargo  movements and handle oil lines as directed by Wharf.
       Ship's fire fighting equipment  must remain operative while at Wharf.
   6.  Potential sources of ignition,  particularly small power craft, should not be allowed
       to approach your Ship  nearer than 100 feet.
   7.  Ship's Officer and Wharf  Representative  shall agree  upon the method of comnunicating
       during cargo movements.   Cargo  movements shall  not begin until the vessel and the
       Wharf inform each other that lines, valves and  tanks are properly set.
   8.  Ver.sel is responsible  for proper  make-up of ship's hose connection, adequate hose
       support.  Avoid hose kinks.   Maintain hose bends  above  12  diameters.
   9.  Tank tops must be kept closed at  all  times.   Ullage  plugs  are to be kept closed at
       all times except when  sampling, thieving or inspecting, at which time they can be
       opened for the necessary  time and then immediately closed.   Tank tops may be open if
       gas free.
* 10.  No ballasting during cargo movements  except when ballast handling Is in a separate
       system from bulk cargo handling.  'Ballast discharge  over side prohibited.  Use shore
       tank only.
   11.  Proper preparation of  tanks  ia  Ship's responsibility.   Consultation Is available.
   12.  Vessel is responsible  for all on  board cargo movements.
   13.  Stnrt loading slowly and  by  gravity when possible.   Top off t«nk by gravity when
       possible.
   lit.  Vessel shall report  Ship's tank gages every 2 hours.
   1^.  ClRss A products shall not be displaced  from cargo hoses with compressed air.
   15.  Scupper plugs shall  be tightly  fitted on the weather deck  in way of tanks before
       cargo or bunker movement  can start.
   17.  Hose limits-.  150°F, 125  psig.
   18.  If contamination or  a  serious leak  is discovered, discontinue the stock moveaent
       until agreement is reached on the proper procedure to follow.
   19.  Your ship must be able to get underway while at Wharf.  Bitter end of mooring lines
       must not be secured.  Fire wires  must be out at bow  and stern.
   20.  No other vessel is permitted to moor  alongside  or allow cargo movements across the
       decks of a Class A vessel.
   ;••   Holler fires shall be  adjusted  so as  to  pre*vnt "Stack  Burnouts".
   '">   Wireless transmission  is  prohibited.   Electrical  repftlr work is  prohibited.
   23.  Handling of ail ship stores  will  be the  responsibility  of  the ship's Officer.
   24   Abide by Federal, State and  Local Air and Water Pollution  Laws.
   25.  Vessel shall provide own  gangway.  Wharf gangway normally  Is not available.

*Revised 3-31-70                         199

-------
                                            -  2  -


  26.  You must  provide your own doctor  or ambulance service.   A local list can be obtained
      from  the  Wharfmaster.
  27.  Keep  both anchors housed.
  28.  Special situations,  such as  repair  work,  require Terminal Executive approval.
  29.  Pedestrians  are not  permitted  on  Long Wharf causeway.   Ride the Company-provided bus.
  30.  Paying passengers cannot board and  must stay aboard your vessel.
  31.  So that shore booster pumps  and manifolds can be properly adjusted to eliminate
      possible  hazards to  these facilities, a 15-mlnute notification shall be given to the
      wharf men in charge  of  the berth  prior  to the:
                       (I)  Stopping  of  any cargo  movement.
                       (2)  Stripping of any tanks during cargo discharge.
  32.  Cover ship's sewer outlet to deflect material into the  water Instead of on the deck.
 *33.  Cleaning  of  ship's tanks and/or butterworthlng alongside wharves Is prohibited.
 *34.  Deck-watch required  at  all times  while  loading/discharging.

I will abide by  the rules and  regulations  as set forth In Operating Standard RE-3110,
"Loading and Discharging Shipa at Manufacturing Terminals", as well as those prescribed by
Law.
SIGNED	         SIGNED
           (BERTH OPERATOR)                           (MASTER OR AUTHORIZED REPRESENTATIVE)
                                                               (NAME OF VESSEL)
                                                      (DATE)                      (TIME)


The" ToTl owing" section of "this* TornTshould bVused Tor special situation's:
       (NAME OF VESSEL)                    '    (DATE)                         (TIME)
Wh.-»rf approval is required before «hlp can steam, wash
   ",as fro* tanks.                                                  (TERMINAL EXECUTIVE OR
                                                                    AUTHORIZED REPRESENTATIV
The freight holds and/or tanks of this, vessel have been                    .
inspected/tested and have been found safe for men Co enter          (MASTER OR AUTHORIZED
and/or work.  (Must be signed before Company personnel can           REPRESENTATIVE)
enter a freight hold or ship's tank.)

Special situations should be listed here.
                                        200

*ReviseJ 3-31-70

-------
STANDARD OIL  COMPAQ OF CALIFORNIA                          VESSEL:
LOJ:C. VTrfAUF/POINT  ORIENT WHARF                               BERTH-'"
RICHMEJD, CALIFORNIA                                        DATE: ~"
Check Hat of  Itens to be dlacussed betvaan the Captain,Chief Kate, Chief Englnocr end Vhcrf-
noster he fore  atnrt of cargo operation.  Oil tranafer nay not start until ell quooclcaa have
been checked off In the "Yes" circle and .attested below.   Each oncoming Whorfaaater end Kate
must sign- '                         '     ''•''' '*   ^        '•  - •    -  '     "•••••         .

1.  Written cargo and bunker orders have been  reviewed  end agreed  upon as to:
    «.  Quantity & Type of Stock   ()       !               e.  Weua Tinpersturo      ()
    b.  Initial  Transfer Rate      (  )                      f.   Anticipated Stoppacoo    ( )
    c.  Maximum Transfer Rate      (  )                      g.   Booster Pimps            ()
    a.  Maximum Line Pressure      (  )

 ?..  The method o£ communication (signaling  practice) between ship and  shore hao  boon
    established.                                                                        / \

 3.  It  lr, understood a IS minute  standby notice to both ship and shore is required
     for .-.hutting down any cargo transfer, except la an  energency.,                      ( )

 /».  Ho  all agree vessel and gangway Is properly secured at  WharfT                      ( )

 5.  All bolted connections between ship  and shore  are full bolted.                     ( )

 f>.   If  a hold-out (displacement)  la  required,  has  the amount and procedure been
     nt;reed-upon?                   .                                                     ^ ^

 7.   In  there a clear understanding at the terminal and on board ship the steps to bo
     taken for containment and  clean-up in the  event of an oil cplll?                   ( )
                                   (-> ~ •. •• >
 >\.   Aro. c.ir^ii/bunker hoses In  good condition?                                           ( )

 9.   Sen r-.iictlon valven will  be-. p:ccp*tiy la«hed and opened only If under  the'direct
     supervision of  the Officer In charge.   Wharfmaater  to be notified  when valves
     opened.                         v  ._, , ,,                                  ,       •    ..  ( )

 10.  HA-J Anv Anticipated  repair work been brought to the Wharfmaater1 s attention?       ( )

 11.  Ship  nn-1 nhore  2-hour  gages  will be exchanged.                          ,           ( )

 12.  Portholes on Wharf side  are  closed or properly icreened.                           ( )

    WHARFMASTER           SHIP'S OFFICER    '   TITLE           SIIIP'S OFFICER      TITLE
  2.                    2.
  3.                    3.                _   _ .      9.
 5. __ _  5.

 6.                    6.
                                            201           ou.S. GOVERNMENT PRINTING OFFICE:1972 484-487/3571-3

-------