SEPA
            United States
            Environmental Protection
            Agency
            Industrial Environmental Research
            Laboratory
            Cincinnati OH 45268
EPA-600 2-80-151
June 1980
            Research and Development
Evaluation of an
Electrostatic
Precipitator for
Control of Emissions
From a Copper
Smelter
Reverberatory
Furnace

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                RESEARCH REPORTING SERIES

Research reports of the Office of Research and Development, U.S. Environmental
Protection Agency, have been grouped into nine series. These nine broad cate-
gories were established to facilitate further development and application of en-
vironmental technology.  Elimination of traditional grouping was consciously
planned to foster technology transfer and a maximum interface in related fields.
The nine series are:

      1.  Environmental  Health Effects Research
      2.  Environmental  Protection Technology
      3.  Ecological Research
      4.  Environmental  Monitoring
      5.  Socioeconomic Environmental Studies
      6.  Scientific and Technical Assessment Reports (STAR)
      7.  Interagency Energy-Environment Research and Development
      8.  "Special" Reports
      9.  Miscellaneous Reports

This report has been assigned to the ENVIRONMENTAL PROTECTION TECH-
NOLOGY series. This series describes research performed to develop and dem-
onstrate instrumentation, equipment, and methodology to repair or prevent en-
vironmental degradation from point and non-point sources of pollution. This work
provides the new or improved technology required for the control and treatment
of pollution-sources to meet environmental quality standards.
This document is available to the public through the National Technical Informa-
tion Service, Springfield, Virginia 22161.

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                                           EPA-600/2-80-151
                                           June  1980
EVALUATION OF AN ELECTROSTATIC PRECIPITATOR FOR CONTROL
OF EMISSIONS FROM A COPPER SMELTER REVERBERATORY FURNACE
                         by
         Grady B. Nichols, Joseph D. McCain,
      James E. McCormack and Wallace B. Smith
            Southern Research Institute
              2000 Ninth Avenue South
             Birmingham, Alabama 35205
                  Grant No. R804762
                  Project Officer

                   John 0. Burckle
       Industrial Pollution Control Division
   Industrial Environmental Research Laboratory
               Cincinnati, Ohio 45268
   INDUSTRIAL ENVIRONMENTAL RESEARCH LABORATORY
        OFFICE OF RESEARCH AND DEVELOPMENT
       U.S. ENVIRONMENTAL PROTECTION AGENCY
               CINCINNATI, OHIO  45268

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                          DISCLAIMER
      This report has been reviewed by the Industrial Environ-
mental Research Laboratory, U.S. Environmental Protection
Agency, and approved for publication.  Approval does not signify
that the contents necessarily reflect the views and policies of
the U.S. Environmental Protection Agency, nor does mention of
trade names or commercial products constitute endorsement or
recommendation for use.
                               li

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                           FOREWORD


     When energy and material resources are extracted, processed,
converted, and used, the related pollutional impacts on our
environment and even on our health often require that new and
increasingly more efficient pollution control methods be used.
The Industrial Environmental Research Laboratory - Cincinnati
(lERL-Ci) assists in developing and demonstrating new and
improved methodologies that will meet these needs both
efficiently and economically.

     This report presents the findings of an investigation of
air pollutant emissions from the reverberatory furnace pollution
control system at a primary copper smelter.  The study was per-
formed to assess the degree of particulate emissions control and
control problems associated with the application of electro-
static precipitators in the nonferrous metals production
industry.  The results are being used within the Agency's Office
of Research and Development as part of a larger effort to define
the potential environmental impact of emissions from this
industry segment and the need for improved controls.  The
findings will also be useful to other Agency components and the
industry in dealing with environmental control problems.  The
Metals and Inorganic Chemicals Branch of the Industrial Poll-
ution Control Division should be contacted for any additional
information desired concerning this program.
                                  David G. Stephan
                                      Director
                    Industrial Environmental Research Laboratory
                                     Cincinnati
                               111

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                           ABSTRACT
     This report describes tests to evaluate the performance
of an electrostatic precipitator installed on a copper rever-
beratory furnace.  Particle size measurements were made with
modified Brink cascade impactors in order to calculate the ESP
fractional efficiency.  The particle size distributions at the
inlet and outlet were both found to be biomodal.  The overall
mass median diameter of the inlet distribution was greater
than 10 urn.  The SRI-EPA computer model was used to simulate
the ESP performance.  Values of the mass collection efficiency
were found by instack filters to be 96.7%, and by cascade
impactors to be 96.6%.  The computer model predicted an overall
efficiency to be 96.8%, which is also the design efficiency.

     The particulate matter was found to be very cohesive and
hygroscopic, and the composition  (color) varied from impactor
stage to stag.e.  There was no evidence of electrical problems
due to particle resistivity or space charge.

     Simultaneous testing was also carried out by Radian
Corporation, Austin, Texas.  Results of the Radian study are
included in a report "Trace Element Study at a Primary Copper
Smelter, Vol. I and II"  (EPA-600/2-70-065a and -065b, March
1978).  An evaluation of another such control system  (installed
at a different smelter) entitled "Performance Evaluation of an
Electrostatic Precipitator Installed on a Copper Smelter
Reverberatory Furnace", EPA-600/2-79-119, was published in
June, 1979.
                               IV

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                           CONTENTS
                                                     s
Foreword	   iii
Abstract	    i v
Figures	    vi
Tables	  viii

  1.  Summary and Conclusions	     1
  2.  Introduction	     3
  3.  Experimental Procedures and Discussion	     4
        Description Of The Electrostatic Precipitator..     4
        Gas Velocity Distribution	     9
        Collection Electrode Design	     9
        Maintenance and Operation	    14
        Particle Size Measurements	    14
  4.  Test Results	    18
        Particle Size Distribtutions	    18
        Particulate Mass Concentration	    32
        Sulfur Oxide Concentration	    32
        ESP Collection Efficiency	    34
  5.  Appendix - Procedures and Data for Impactor Tests    38
        Brink Impactor Operating Procedures	    38
        Data	    42

References	    63

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                             FIGURES
Number
                                                             Page

  1    Approximate Dimensions of the Active Area of the
        Electrostatic Precipitator	  5

  2    Circuits Used to Measure Electrical Operating
        Characteristics of the Electrostatic Precipitator....  7

  3    Voltage-Current Characteristics of the Three ESP
        Power Sets	13

  4    Sampling setup for the Brink Impactor using redundant
        calibrated orifice flowmeters	15

  5    Plot of Aerodynamic Diameter (Density =1.0 gm/cm3)
        versus Physical or Stokes Diameter  (Density = 3.58
        gm/cm3)	17

  6    Inlet Particulate Loading Versus Particle Diameter
        on July 9 at 0720 HRS in Port 4 of West Pantleg	19

  7    Inlet Particulate Loading Versus Particle Diameter
        Measured on July 9 at 1200 HRS in Port 4 of East
        Pantleg	20

  8    Inlet Particulate Loading Versus Particle Diameter
        Measured on July 9 at 0700 HRS in Port 3 of West
        Pantleg	21

  9    Inlet Particulate Loading Versus Particle Diameter
        Measured on July 9 at 1135 HRS in Port 3 of East
        Pantleg	22

 10    Inlet Particulate Loading Versus Particle Diameter
        Measured on July 10 at 0640 HRS in Port 3 of East
        Pantleg	23

 11    Inlet Particulate Loading Versus Particle Diameter
        Measured on July 10 at 1000 HRS in Port 3 of West
        Pantleg	24

 12    Outlet Particulate Loading Versus Particle Diameter
        Measured on July 9 at 0720 HRS in Port 1	25

 13    Outlet Particulate Loading Versus Particle Diameter
        Measured on July 9 at 1500 HRS in Port 3	26


                                vi

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                         FIGURES (Cont'd.)
Number                                                       Page

 14    Outlet Particulate Loading Versus Particle Diameter
        Measured on July 10 at 0635 HRS in Port 3	  27

 15    Average Cumulative Mass Loading Versus Particle
        Diameter for all Inlet Impactor Tests	  28

 16    Average Cumulative Mass Loading Versus Particle
        Diameter of all Outlet Impactor Tests	  29

 17    Inlet Size Distribution on a Cumulative Percentage
        versus Particle Size Basis	  30

 18    Outlet Size Distributions on a Cumulative Percentage
        versus Particle Size Basis	  31

 19    Measured and Theoretical Fractional Efficiency Curves
        for the Electrostatic Precipitator	  36
                               VII

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                            TABLES





Number



  1   Electrostatic  Precipitator Descriptive Parameters

2
3

4

5

6
7
8
9
For A Reverberatory Furnace 	 	 	
Power Supply Log, Reverberatory Furnace, ESP 	
Voltage Vs. Current Values For Electrostatic
Precipitator. Power Set A. . . 	
Voltage Vs. Current Values For Electrostatic
Precipitator. Power Set B 	
Voltage Vs. Current Values For Electrostatic
Precipitator. Power Set C 	
Mass Concentration and Efficiency 	
Sulfur Oxide Concentration 	
Overall Mass Collection Efficiency 	
Brink Impactor Blank Runs 	 	 	 	 	
6
8

10

11

12
33
34
37
43
10-27 Cascade Impactor Data	   45-62
                             Vlll

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                          SECTION 1

                   SUMMARY AND CONCLUSIONS


      Tests were performed on July 9 and 10, 1976 to measure the
fractional collection efficiency of a Joy-Western Precipitation
electrostatic precipitator installed on a copper reverberatory
furnace.

      From qualitative observations of cascade impactor stage
catches it was determined that the particulate emissions are
very cohesive, hygroscopic, and very likely inhomogeneous in
composition with respect to particle size.  The mass median
diameter of the inlet particle size distribution was greater
than 10 ym.  The inlet particle size distributions were bimodel
with one component having a mass median diameter less than 1 ym.

      The electrical operating data indicate that the ESP was
in good mechanical alignment and electrical condition.  The
overall collection efficiency, measured by instack filters
operating at stack temperatures (^300°C) was 96.7%.  The overall
collection efficiency calculated from cascade impactor data was
96.6%.  The theoretical collection efficiency, predicted by the
SRI-EPA computer model, was 96.8%.  The design efficiency was
96.8%.

      A potential source of trouble with the application of ESP's
to sources of very fine particulate is suppression of the corona
current by a particulate space charge.  Although some reduction
in current was observed at the ESP inlet, the degree of suppres-
sion was not large.  This can be attributed to the fact that
the particles were larger than expected, and the concentration
was rather low.

1.  The mass collection efficiency at gas conditions agreed
    with the theoretical and expected behavior of the device.
    The measured efficiency and design efficiency were identical
    within experimental error.

2.  The power supply voltage vs current characteristics suggest
    that the electrode system was in good mechanical alignment.

3.  Particulate resistivity was not limiting the operating
    characteristics of the collector.

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4.  The gas velocity distribution, as reported by Radian, was
    good in the inlet and outlet sampling planes.

5.  There was an apparent difference in the chemical composition
    with respect to particle size.

6.  A significant variation in sulfur oxide concentration
    occurred with time.

7.  No significant change in electrostatic precipitator opera-
    tion was deemed to be necessary for optimal operation.

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                          SECTION 2
                         INTRODUCTION
      Southern Research Institute worked in cooperation with
the Radian Corporation to evaluate the performance of an elec-
trostatic precipitator installed on a copper reverberatory
furnace.  In this particular test, Southern Research personnel
conducted measurements of the inlet and outlet particle size
distribution and voltage-current characteristics of the elec-
trostatic precipitator.  A computer simulation of the ESP
performance was made using the computer systems model developed
at SRI under the sponsorship of the EPA Industrial Environmental
Research Laboratory at Research Triangle Park, N.C.

      Section 3 contains a description of the ESP and a dis-
cussion of the experimental procedures which were used to make
measurements of the particle size distributions.  Section 4
contains reduced data from the particle size distribution
measurements, and a comparison of the measured efficiency with
that predicted by the computer model.  All of the data taken
with the Brink impactors is contained in Section 5, the Appendix.
Section 5 also contains a more detailed summary of the proce-
dures which were used to obtain particle size information with
the Brink impactors.

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                           SECTION  3

            EXPERIMENTAL PROCEDURES AND DISCUSSION


DESCRIPTION OF THE  ELECTROSTATIC PRECIPITATOR

      Figure  1 is a schematic which shows the overall dimensions
and electrical sectionalization of the Joy-Western electrostatic
precipitator  (ESP)  used to control the emissions from a reverb-
eratory furnace.  Table 1  summarizes the descriptive parameters
of the ESP.

      The electrostatic precipitator is physically divided in
the center such that two independent gas flow paths are provided.
No data are available pertaining to turning vanes, baffles or
gas distribution plates.

      The power supply control cabinets are equipped with pri-
mary voltage  and current meters.   Measurements of the secondary
voltage values were made by installing temporary voltage divi-
ders.  Series resistors of 26ft, previously installed by Joy-
Western, were used  to monitor the  currents.  The circuits used
to measure the secondary currents  and voltages are shown in
Figure 2.

      Operating values for the primary and secondary currents
and voltages  were monitored throughout the tests.  Power set C
was operated  in the manual mode because the automatic control
system was inoperative.  The manual settings were kept at near
optimum values during the  tests by SRI personnel.  Sets A and B
were operated in the automatic mode.  At the conclusion of the
particulate collection efficiency  tests, complete V-I character-
istics were measured for all three electrical power sets.
(Repair to power set C would have  caused a delay in the test
program).

      Values  for the operating current and voltage which were
recorded during the efficiency tests are shown in Table 2.
These values  were recorded at approximately 1 hour intervals,
but for periods where the  input power did not fluctuate from
the average by more than five percent, only the average is
included.

      The electrical operating data indicate that the ESP was
in good condition.   Although the inlet section, set C, could

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                                                            FLOW
Figure 1.  Approximate Dimensions of the Active Area of the
           Electrostatic Precipitator

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(Ti
              TABLE  1.   ELECTROSTATIC PRECIPITATOR DESCRIPTIVE PARAMETERS
                                      FOE A REVERBERATORY FURNACE
                      ITEM
                                            ENGLISH
           Collection electrode area (A)(total-2 ESP) 39744 ft'
  Inlet set area  (power set C)
  Outlet set area  (power set A)
  Outlet set area  (power set B)
Collection electrode spacing
Corona electrode diameter  (round wire)
Collection electrode dimension
Number of gas passages (total - 2 ESP)
Gas passage length  (active)
Volume flow rate design  (V)*
Design temperature
Design efficiency
Design precipitation rate parameter   (w)
Specific collection electrode area  (A/V)
  19872  ft2
   9936  ft2
   9936  ft2
     9 in.
  0.1055 in.
)  ft  x 24 ft
     46
   18 ft
150,000 acfm
  600-700°F
   96.83%
0.21 ft/sec
265  ft2/thousand
     cfm
 METRIC
 3692.4  m2
 1846.2  m2
 923.0  m2
 923.0  m2
 0.229  m
   2.7 mm
>.74 x 7.32  m

   5.49  mm
 70.8 m3/sec
 315-371°C
                                                                     6.5 erf/sec
                                                                       52 m2/m3/sec
          * Note - these conditions were within 5% of the actual measured flows during
           	     the test period.  The temperature and efficiencies were approxi-
                   mately the same.

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               -{
               ~l
CONTROL
                                           TO
                                           VOLTMETER
                                           FOR
                                           VOLTAGE
                                        6.2K
                               50M
       RECI
r*
                           TRANSFORMER
                        TO
                        VOLTMETER -*-
                        FOR
                        CURRENT
                                   26 A
                                             RECTIFIERS
                                               E.S.P.
                          S.A =
                          SURGE ARRESTOR
         1.  SECONDARY VOLTAGE = V, X 5° X 1° + 6-2 X 10
                                  6.2 X 10
                            V2
                             8.1 X 10 V,
         2.  SECONDARY CURRENT =
                            26
Figure 2.   Circuits Used to Measure Electrical Operating
           Characteristics of the Electrostatic Precipitator

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              TABLE 2.  POWER SUPPLY  LOG,  REVERBERATORY FURNACE,  ESP
oo


Date Time Set
7-8-76 7:00 A
B
C
7:10 A
B
C
9:00-10:40 A
B
C
11:30-1:00 A
B
C
7-9-76 7:00-1:00 A
B
C
7-10-76 5:00-7:30 A
B
C
8:00 A
C
C
8:07-12:00 A
B
C
Voltage,
Primary
(KV)
210
220
260
230
280
280
250
290
290
245
280
290
260
290
290
250
285
280
240
255
280
265
300
300
Current,
Primary
(V)
80
70
90
125
175
135
160
165
140
155
.165. '
135
155
165
110
155
165
120
125
125
120
165
170
155

Power
(kW)
16.8
15.4
23.4
28.8
49.0
37.8
40.0
47.9
40.6
38.0
46.2
39.2
40.3
47.9
31.9
38.8
47.0
33.6
30.0
31.9
33.6
43.7
51.0
45.0
Voltage ,
Secondary
(kV)
32.0
32.5
36.0
33.5
36.3
36.4
35.5
36.8
37.1
35.0
36.0
37.1
36.5
36.8
37.3
35.0
37.5
37.0
34.5
35.5
37.0
36.5
38.5
38.5
Current,
Secondary
(mA)
231
261
281
378
584
420
515
600
505
480
560
505
530
579
393
543
552
408
409
386
408
562
571
556

Power
(kW)
7.4
8.5
10.1
12.7
21.2
15.3
18.3
22.1
18.7
16.8
20.2
18,7
19.3
21.3
14.7
19.0
20.7
15.1
14.1
13.7
15.1
20.5
22.0
21.4

Current
MA/ ft2
24.0
27.0
14.9
40.1
61.9
22.3
54.6
63.6
26.8
50.9
50.9
26.8
56.3
61.4
20.8
57.5
58.5
21.6
43.3
40.9
21.6
59.6
60.5
29.5

Density
mA/m2 Comments
.25
.28
. 15
.41
.63
.23
.56
.65
.27
.52
.61
.27
.57
.63
.21
.59
.60
.22
.44 Upset relates to
.42 charging furnace
.22
.61 Normal
.62
.30

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only be operated at a considerably lower current density than
the outlet section sets A and B-;- this behavior is normal and can
be explained in terms of a space charge effect.  For cases of
moderate and heavy mass loading,, a space charge consisting of
charged fine particles exists in the interelectrode space and
causes a suppression of the corona current.  Downstream sections
are subjected to a lower concentration of uncollected particu-
late and usually can be operated at higher current densities.

      The power supply designs were considered to be adequate
in that the automatic control system operated with some sparking
at currents below the current rating of the power supplies.  The
TR Set ratings are 1100 ma for sets A and B and 1400 ma for set
C.  Therefore, the power supply-"ratings were adequate.

      The current suppression related to the space charge effect
can be explained in terms of a reduced effective mobility of the
charge carriers.  If the entire current is carried by gas mole-
cules, then the total current flow is caused by ionic motion.
However, when significant electrical charge is attached to
particulate matter, the velocity of which is much less than that
for ions, the phenomenon of space charge suppression of current
occurs.

      Tables 3,4, and 5, and Figure 3 contain data showing the
complete voltage-current characteristics for the ESP.  Again,
these curves are normal, and show no indication of any high
resistivity problem nor a severe space charge problem.

GAS VELOCITY DISTRIBUTION

      It was initially intended to conduct gas velocity distri-
bution measurements within the internal portion of the electro-
static precipitator.  It was not possible to make this measure-
ment because the anticipated reverberatory furnace shutdown did
not occur.  Therefore, the on^.y gas velocity measurement was
made in the inlet and outlet plenum areas.  These data were
reported by Radian.

      The computer system projection suggested that the gas
velocity distribution within the'unit was acceptable.

COLLECTION ELECTRODE DESIGN

      No discussion was included about the specific design of
the collection electrode system.  No data were available that
could be used to show that any particular electrode design is
superior to another.

      Each individual equipment supplier provides the design
that they feel best applies to their device.   In the absence
of definite supporting data, np general comment was warranted

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         TABLE 3.  VOLTAGE VS. CURRENT VALUES FOR ELECTROSTATIC PRECIPITATOR

                             INSTALLED ON A REVERBERATORY FURNACE
H
o

(Plate
area
9936 ft2
)




Power Set A
Vpri (V)
260
250
225
200
185
175
160
150
125
100
pri(A)
170
150
110
75
50
40
30
25
10

Power
44.
37.
24.
15.
9.
7.
4.
3.
1.

(kW)
2
5
8
0
3
0
8
8
3

V
sec
36
35
33
31
29
29
28
26
23
22
(kV)
.5
.5
.0
.2
.6
.2
.1
.5
.7
.3
sec(mA)
573
515
344
212
131
102
67
40
9
3
Power (kW)
20
18
11
6
3
3
1
1
0

.9
.3
.4
.6
.9
.0
.9
.0
.2

Eff %
47
49
46
44
42
43
39
28
17

Current
]iA/ft2
57.7
51.8
34.6
21.3
13.2
10.3
6.7
4.0
0.9
0.3
Density
mA/m2
.62
.56
.37
.23
.14
.11
.07




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TABLE 4.  VOLTAGE VS. CURRENT VALUES  FOR ELECTROSTATIC PRECIPITATOR
                    INSTALLED ON A REVERBERATORY FURNACE

(Plate area 9936 ft2)
Power
Vpri(V) :
290
275
250
235
225
200
185
175
145
125
100
Cpri(A]
175
167
120
90
65
40
30
20
10
0

I Power
50.
45.
30.
21.
14.
8.
5.
3.
1.


(kW)
7
9
0
1
6
0
5
5
5


sec
36.
36.
33.
32.
31.
29.
28.
28.
24.
23.
19.
Set
(kV)
8
1
8
1
7
9
8
5
4
1
8
B
sec (mA)
621
565
378
285
254
148
107
86
21
14
4

Power
22.
20.
12.
9.
8.
4.
3.
2.
0.



(kW)
9
4
8
1
1
4
1
5
5



Eff %
45
44
43
43
55
55
56
70




Current
yA/ft2
62.5
56.9
38.0
28.7
25.6
14.9
10.8
8.7
2.1
1.4
0.4

Density
mA/m2
.67
.61
.40
.31
.28
.16
.12
.09




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TABLE 5.  VOLTAGE VS. CURRENT VALUES FOR ELECTROSTATIC PRECIPITATOR
                    INSTALLED ON 'A REVERBERATORY FURNACE
(Plate area 19872 ft2)
Power Set
Vpri(V) :
320
300
H 275
(0 * '3
250
225
200
175
160
125
100
Epri (A)
190
160
110
75
45
25
10
0


Power (kW)
60.8
48.0
30.2
18.8
10.1
5.0
1.75



Vsec(kV)
39.0
37.8
36.1
34.7
33.4
32.0
29.8
28.3
23.5
17.5
C
sec(inA)
730
585
379
235
135
68
32
15
5
1

Power (kW) Eff
28.5 47
22.1 46
13.7 45
8.2 43
4.5 45
2.2 44
1.0 54




Current
% pA/ft2
36.79
29.4
19.1
11.8
6.8
3.4
1.6
0.8
0.2
0.05

Density
mA/m2
.40
.32
.21
.13
.07
.04
.02




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   0.70
   0.60
   0.50
 I
 E 0.40
 LLJ
 Q
 \-

 1 0.30
 oc
 o
   0.20 -
   0.10 —
         • POWER SET A
         • POWER SET B
         A POWER SET C
                                         ^m
                                        I
                 10          20          30
                   SECONDARY VOLTAGE. kV
                                      40
Figure 3,
Voltage - Current Characteristics  of the
Three ESP Power Sets
                           13

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for an individual design.

MAINTENANCE AND OPERATION

      The behavior of the electrostatic precipitator was con-
sidered to be good.  The plant had a maintenance man assigned
to the Electrostatic Precipitator Control Room.  He repeatedly
checked the power supply readings and noted the general condi-
tions of the unit.  The material collected by the electrostatic
precipitator was moved by screw conveyors into a storage bin for
recycling through the smelter.  No particular problems were
noted with the system.

      The particular maintenance and operation program that is
followed by individual plants is formulated between the equip-
ment user and supplier.  These programs range from complete
inspection and repair carried out at specified intervals to no
maintenance work until a significant failure occurs.  In many
cases, electrostatic precipitators may operate satisfactorily
for several years with little or no maintenance required while
in others-, extensive maintenance is required.  Each supplier
and user decides what is correct for each installation.  The
program followed at the test smelter seemed to be adequate
because the electrostatic precipitator appeared to be in good
operating condition.

PARTICLE SIZE MEASUREMENTS

      Cascade impactors were used to measure the size distribu-
tion of particles suspended in the flue gas at the ESP inlet
and outlet in order to characterize the particulate and to
measure the collection efficiency vs. particle size.  Brink
cascade impactors, modified and calibrated at SRI, were chosen
for this application because their low sampling rate allows
longer sampling times and better averaging of emissions during
process changes.  Figure 4 shows the sampling train that was
used during these tests.

      On-site pretest investigations were done during the week
of June 28 in order to determine the extent to which gas phase
reactions between the rather high SOX constituent of the efflu-
ent gas and glass fiber collection substrates and filters might
interfere with the tests.  The results from these tests indicate
that the Reeve Angel 934AH material was sufficiently inert to
allow confidence in the subsequent test data.  A secondary pur-
pose of the pretest was to provide an estimate of the sampling
time required to obtain a weighable sample without overloading
the impactor stages.  Data for the efficiency tests were
obtained on July 9 and 10.

      Section 5, the Appendix, contains a more detailed descrip-
tion of the procedures that were used to collect impactor samples,

                              14

-------
     PROBE
    -5
                                        DRYING
                                        COLUMN
                 PORT
                                                                 HEAT EXCHANGER
  IMPACTOR
AIR
FLOW
U METERING METERING
\X^ TEE ORIFICE ORIFICE
^=1
/
Hg MANOMETER
)/
ifcli


—

—
~J 	 Pi IMP

=>I20 MAWMETER3
           Figure 4.
Sampling setup for the  Brink  Impactor using redundant
calibrated orifice flowmeters.

-------
and all of the data are tabulated there.

      The term "particle size" is somewhat ambiguous if the
particle shape is irregular, or if the mass density is unknown
or inhomogeneous.  Fortunately, many particles created by con-
densation are spherical and the diameter is used to measure
size.  If the particles are spherical, and the density is known,
cascade impactors yield information on the actual physical size.
If the shape and density are unknown,  particle size is generally
reported in terms of "aerodynamic diameter".  The aerodynamic
diameter of a particle is related to its behavior in a gas and
is defined as the diameter of a sphere of unit density with the
same settling velocity as the particle of interest.  Cascade
impactors measure the aerodynamic diameter directly. (See the
Appendix for detailed discussion).

      Since the aerosol of interest was a condensation product,
and an approximate density of 3.58 gm/cm3 was given by the
plant personnel, all the particle size distributions reported
here are based on the physical or Stokes diameter. Figure 5
is a curve relating aerodynamic diameters to physical diameters
for a mass density of 3.58 gm/cm3.  This curve can be used to
change any of the particle diameters reported here to an
aerodynamic basis.
                               16

-------
  10'
II
Q.


o
IT
UJ
  10°
  10"1
         51
               inin
                                       -rrt!
                                                      r 1
    10
      -1
10°
                                                         10
                                                                                   10'
                              ESTIMATED PHYSICAL DIAMETER, micrometers
             Figure 5t  Plot of Aerodynamic Diameter (Density = 1.0  gm/cm3)
                        versus Physical or Stokes  Diameter  (Density  =  3.58
                        gm/cm3).
                                        17

-------
                           SECTION  4

                          TEST  RESULTS
PARTICLE  SIZE  DISTRIBUTIONS

      Six measurements  of  the  particle  size  distribution were
made at the  inlet  and three  at the  outlet  during thest tests.
The inlet data are shown plotted as cumulative mass  loading
vs. particle diameter in Figures 6  through 11 and the outlet
data in Figures 12 through 14.   Although the impactors have no
size resolution above ten  micrometers,  a single point is shown
at the extreme right hand  side of each  graph.  This  corresponds
to the total particulate mass  loading measured by that test.
The data  for the first  outlet  run,  shown in  Figure 12, is of
questionable validity because  the filter and substrates for
this test were found to be wet upon dissassembling the impactor.
This probably  occurred  as  a  result  of condensed water within
the probe accidentally  running back into the impactor after it
was removed  from the duct.

      Figure 15 shows the  averaged  inlet size distribution
plotted as cumulative mass versus particle diameter.  Figure 16
shows the averaged outlet  data.   Figures 17  and 18 are the
averaged  inlet and outlet  size distributions plotted as cumula-
tive percent of the total  particulate loading versus particle
diameter.

      The averaged particle  size distributions are all plotted
with 90%  confidence limits shown.   The  confidence limits are
rather large,  primarily for  three reasons: 1) there were a small
number of samples  taken, 2)  the source  fluctuations  introduced
scatter/and  3)  the collected particles  clung together to form
conical deposits underneath  the impactor jets.  These deposits
quickly grew large enough  to plug the jets if sampling times
were too  long.   Thus, smaller  sampling  times than desirable
were used and  the  weighing accuracy was limited.

      The inlet distribution is bimodal with a fine  particle
mode having  a  mass median  diameter  of approximately  0.8 micro-
meters.   Approximately  22% of  the mass  is  contained  in particles
with diameters smaller  than  10  micrometers.  The overall mass
median diameter of the  inlet particle size distribution is
greater than 10 micrometers.


                               18

-------
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      icr1             10°              lo1

            PARTICLE DIAMETER (MICROMETERS)
       Figure 6. Inlet Particulate Loading Versus Particle

                Diameter Measured on July 9 at 0720 HRS in Port

                4 of West Pantleg.  Density = 3.58 gm/cm3.
                               19

-------
                                                            TlO1
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             PARTICLE DIAMETER  (MICROMETERS)
         Figure 7. Inlet Particulate Loading Versus Particle
                  Diameter Measured on July 9 at 1200  HRS in
                  Port 4 of East Pant leg.  Density = 3.58 gm/cm3

                                20

-------
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PARTICLE DIAMETER  (MICROMETERS)
H	1  I  I I I III
                                                          id5
          Figure 8.  Inlet Particulate Loading Versus Particle

                   Diameter Measured on July 9 at 0700 HRS in

                   Port 3 of West Pantleg.  Density = 3.58 gm/cm3.



                                 21

-------
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             PARTICLE  DIAMETER  (MICROMETERS)
           102

             I
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                                                                  CD
          Figure 9. Inlet Particulate Loading Vers-os Particle

                   Diameter Measured on July 9 at 1135 HRS in

                   Port 3 of East Pantleg.  Density = 3.58 gm/cm3.
                                22

-------
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                                        101
             PARTICLE DIAMETER  (MICROMETERS)
1—I  MINI
                             102
          Figure  10» Inlet Particulate Loading Versus Particle

                    Diameter Measured on July 10 at 0640 HRS

                    in Port 3 of East Pantleg.  Density = 3.58

                    gm/cm .


                                23

-------
                                                             TlO1
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          Figure  11. Inlet Particulate Loading Versus Particle

                    Diameter•Measured on July 10 at 1000 HRS in

                    Port 3 of West Pant leg.  Density =  3.58 gin/cm3

-------
                                                           -icr1
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       PARTICLE DIAMETER  (MICROMETERS)

   Figure 12. Outlet Particulate Loading  Versus Particle
            Diameter Measured on  July 9 at 0720 HRS in
            Port 1.  Density•= 3.58 gro/cmj. -

                          25
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       PARTICLE DIAMETER  (MICROMETERS!)


     Figure 13.  Outlet Particulate Loading Versus Particle
               Diameter Measured on July 9 at 1500 HRS in
               Port 3. Density of 3.58 gm/cm3.

                          26
                                                          10s

-------
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      ID"1             10°              101              10s
            PARTICLE DIAMETER  (MICROMETERS)
        Figure 14.  Outlet Particulate Loading Versus Particle

                  Diameter Measured on July 10  at 0635 HRS in

                  Port 3.  Density = 3.58 gm/cm3.


                                27

-------
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       PARTICLE DIAMETER  (MICROMETERS)

Figure 15 Average Cumulative Mass Loading Versus Particle
         Diameter for all Inlet Impactor Tests.
                       2B

-------
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        Figure 16 Average Cumulative Mass Loading Versus  Particle

                 Diameter for all Outlet Impactor Tests.
                             29

-------








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       PARTICLE DIAMETER  (MICROMETERS)
  Figure 17  Inlet Size Distribution on a Cumulative
           Percentage versus Particle Size Basis.
                     30

-------






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    PARTICLE DIAMETER  (MICROMETERS)

Figure 18  Outlet Size Distributions on a Cumulative
         Percentage versus  Particle Size Basis.
                  31

-------
  —   Curves are fitted through the data points as shown in
Figures 6 through 14 in order to permit automatic  calculation
of averages and the fractional efficiency.  The computer data
analysis also yields tabular data and this is contained in
Section 5.

      During the tests it was observed that some of the impactor
catches appeared to be hygroscopic.  This was indicated by rapid
weight increases of the various impactor stage catches when the
samples were removed from desiccators.  Also, the color of the
particles was different from stage to stage within the impactor,
indicating that the chemical composition of the particles was
inhomogenuous with respect to size.  If this is true, the value
of 3.58 gm/cm3 which was used to calculate the particle sizes
may not really be appropriate for the entire range of sizes.
Recent research conducted by the Kennecott Copper Corporation
suggests that the particles contained in the aerosol effluent
from copper smelters consists of at least two fractions, a one-
to-ten micrometer size refractory dust and a less-than-one
micrometer component of "sticky" condensation fume.1  Thus, it
is probable that the composition, size and concentration of the
aerosol all change with time.  Under such conditions, long term
sampling or suitable averaging of the data is necessary to
obtain data which accurately represent the emissions.

PARTIUCLATE MASS CONCENTRATION

      In addition to the particulate mass concentration measure-
ments made with cascade impactors by SRI personnel, the Radian
Corporation test personnel made measurements concurrently using
instack filters.  A summary of these data are included in
Table 6.  In general, impactor data are less reliable than
mass trains for obtaining mass concentration data because of
the inability to do isokinetic traverses.  The degree of
agreement between the averaged impactor data and the mass trains
which is shown in Table 6 is normal for sources where the
emissions and gas velocity are not stable.

      The mass emission data were provided by the Radian Corp-
oration from tests conducted simultaneously with those by S.R.I.
Our analyses were based on inlet and outlet loadings with terms
of mass per unit volume.  The total emission in pounds per hour
determined from the Radian test is 12 pounds per hour.  These
data are found in EPA Report 600/2-78-065a & b, "Trace Element
Study at a Primary Smelter".

SULFUR OXIDE CONCENTRATION

      Sulfur oxide samples were collected at the outlet of the
electrostatic precipitator on August 9 and 10, 1976.  The sam-
pling system consisted of a heated, glass-lined sampling probe
with a quartz wool filter, a condenser, and a fritted bubbler

                              32

-------
                             TABLE 6. MASS  CONCENTRATION AND EFFICIENCY
UJ
        DATE
MASS CONCENTRATION
                      Inlet
                     mg/DSCM
                Impactor   Mass Train
                  Outlet
                 mg/DSCM
            Impactor   Mass Train
                                                                    EFFICIENCY
Impactor   Mass Train
        7/9/76

        7/10/76
1146
641
1407
1304
41
21
48
41
96.4
96.7
96.6
96.8

-------
 containing a 3% hydrogen peroxide solution.   A dry test meter
 preceded by a Drierite tower was used to measure the volume  of
 stack gas sampled.

       The water-jacketed condenser was maintained at a tempera-
 ture of 60 to 90°C to remove the sulfuric acid from the gas
 stream while passing the sulfur dioxide and  water vapor.   The
 sulfur dioxide was absorbed and converted to sulfuric acid in
 the peroxide bubbler.  An acid-base titration with O.lN NaOH and
 brom-phenol blue indicator was used to determine the sulfuric
 acid content of each sample.

       Since the sulfur oxide content of the  stack gas might  be
 expected to vary during a charging cycle, an attempt was made
 to collect samples immediately before and after the furnace
 was charged.  The results are shown in Table 7.
 	TABLE 7.   SULFUR OXIDE CONCENTRATION	


         Sampling Rate      Furnace Charge       % By Volume
Date         1/min               Cycle
'/9 3.2
2.9
?/10 2.4
1.9
1.0
after
before
after
before
after
1.0
0.42
0.73
0.63
1.7
0.024
0.019
0.018
0.025
0.067

       Based on very limited data, it appeared that sulfur  oxide
 concentrations in the stack gas were highly variable.   Since  the
 efficiency of the condenser had not been previously evaluated in
 this type of environment, the reliability of the SO3 data  cannot
 be verified.  There was no reason to suspect the accuracy  of  the
 SOa measurements, however.

       There is some question as to the applicability of this
 method to the nonferrous metal industry, as it is currently
 used.   The indicated SO3 concentration appears to be somewhat
 dependent upon the sampling rate, suggesting that perhaps
 insufficient retention time is allowed in the condenser for the
 significantly higher SO3 concentration than encountered in power
 station effluent gas streams.


 ESP COLLECTION EFFICIENCY

       ESP collection efficiency is normally reported two ways.
 The overall mass efficiency, irrespective of particle size, is
 frequently used for purposes of design and guarantees.


                               34

-------
Fractional efficiency, or efficiency versus particle size, is
more meaningful for research and development purposes because
both theories and experiments indicate a strong dependence of
efficiency upon the particle size distribution.  In general, one
expects a "U shaped" fractional efficiency curve with a minimum
near 0.2 or 0.3 ym diameter.

      Figure 19 shows measured and calculated fractional effi-
ciency curves for the Joy-Western ESP.  The theoretical curve
was generated by the SRI-EPA computer model, which was developed
under Contract No. 68-07-0265.  Averaged "normal" operating
conditions of the ESP for this specific installation were used
as input data.  The theoretical curve shown in Figure 19 was
predicted for ideal conditions; i.e., no corrections were made
for rapping losses, poor velocity distribution, or gas bypassing
the active areas.

      Rapping reentrainment losses are an important nonideal
feature of full scale ESP behavior and normally constitute a
substantial percentage of the penetration.  As previously men-
tioned, however, the particles caught on the impactor stages
tended to adhere to one another, forming large agglomerates.
Agglomeration on the ESP plates would minimize rapping losses
and justifies our approximation of neglecting such losses in
the computer simulation.

      The experimental points in Figure 19 were taken from the
averaged inlet and outlet particle size distributions.  The con-
fidence limits were calculated in such a way as to represent
outer bounds.

      The fractional efficiencies indicated in Figure 19 com-
pares the measured with that computed from the ESP model.  The
ESP model did not include any estimate for rapping entrainment.
Therefore, the material reentrained during rapping is expected
to consist of agglomerates of previously collected material.
There is a discrepancy between the measured and predicted values
for particles  larger than about 3-5 microns.  This is indicated
by the hyphen predicted efficiency for particles larger than
about 5 microns.

      The measured and calculated overall mass collection effi-
ciencies are shown in Table 8.  The agreement along the measured,
calculated, and design efficiencies indicated that the ESP was
performing well.

      One can also dedupe that the particulate emissions from
this copper smelter present no resistivity problems.  Rapping
losses are not yet defined.  It was not possible to assess the
potential impact of space charge suppression of the corona by
fine particles because the emissions were, on the average, rather
low in particulate concentration.

                               35

-------
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      PARTICLE DIAMETER  (MICROMETERS)

Figure 19  Measured and Theoretical Fractional Efficiency
          Curves for the Electrostatic Precipitator.
                        36

-------
  	TABLE 8.  OVERALL MASS COLLECTION EFFICIENCY	

    Mass Trains                      Computer
   (Radian Corp.)     Impactors      Simulation       Design


      96.7%             96.6%            96.8%         96.8%
      The total emissions from a reverberatory furnace consist
of particulate and gaseous emissions.  The electrostatic pre-
cipitator is only useful for collecting particulate matter with
a significant collection efficiency.  Therefore, only that
material that exists as a particulate is expected to be collected
by the device.  Any material that exists in the gas phase at the
operating temperature of the electrostatic precipitator will
pass through the unit with essentially no removal.

      Therefore, the collection efficiency measured for a given
installation will depend upon the type of measurement system
utilized.  If the purpose for the study is to determine the
operating characteristic of a control device, the measurement
should be made with instrumentation operating at the gas condi-
tions.  This assures that the mass loading and particle size
distribution data represent the conditions that exist in the
control device.  This measurement, however, provides no infor-
mation about condensables or what might be particulate at other
conditions of temperature and pressure.

      The analysis presented in this report is based on the in-
stack measurement conditions since the purpose for the test was
to evaluate the control device.  The total emissions, determined
by the Radian Corporation, are included in a report "Trace
Element Study at a Primary Copper Smelter,  Vol.  I and II"  (EPA-
600/2-70-065a and -065b, March 1978).
                              37

-------
                           APPENDIX

            PROCEDURES AND DATA FOR IMPACTOR TESTS


BRINK IMPACTOR OPERATING PROCEDURES

Pretest

      Before every test of an unfamiliar source, it is SRI's
practice to perform preliminary testing.  Surveys of the site
are made in order to determine the accessibility and suitability
of sampling ports, platforms, and electrical power.  Provisions
are made for any special adapters or sampling procedures.
Approximate mass loadings are determined, and potential sub-
strate reactions with the flue gas are checked.  Such interfer-
ing reactions can cause weight changes in the substrates and
backup filters and thus confuse the results from particulate
catches.

      During the pretest period, both blank and particulate
impactor tests were made.  For blank runs the impactors are pre-
pared as in an actual run except that a Gelman 47mm filter
holder with glass fiber filter is attached to the impactor inlet.
The impactor is then inserted into the sampling port and opera-
ted as if a normal particle size distribution measurement were
being made. After the run the impactor is disassembled, the
substrates are removed, examined, desiccated for 24 hours, and
weighed.  The observed weight gains  from these tests and blank
tests made during the main test period are used as quality con-
trol monitors for the particulate sampling runs.

Sampling Procedures—

      Modified Brink cascade impactors were used at the ESP
inlet and outlet.  The Brink impactor was selected because its
low flow rate allows relatively long sampling times, long
enough in this instance to sample throughout at least one fur-
nace cycle.  Our procedures are specific for this test and
could be slightly different for other sources.

      The impactors were purchased from Monsanto Envirochem as
five stage units.  We have designed and added a precollector
cyclone and two additional stages.  Also, we always operate the
impactors at a flowrate which is much lower than the manufac-
turer's design flowrate.  No cyclones were used at the ESP

                               38

-------
outlet because of the relatively low concentration of large
particles.

      Impactor flowrates cannot be modulated during a test to
maintain isokinesticity, thus traverses were approximated by
taking discrete samples at several points in the ducts.  The
nozzle diameters were selected so that the sampling velocity
was equal to the average flue gas velocity at the particular
sampling point.  Redundant orifice meters were used to set and
monitor the sample flowrate, as shown in Figure 4.

      Normally, the length of the sampling time is dictated by
the mass loading and particle size distribution.  Tests subse-
quent to the first have sampling times adjusted such that no
single stage, excluding a cyclone  if one is used, contains more
than 10 mg. of mass.  For these tests, however, the sampling
times were cut short by particle buildup which plugged the
impactor jets, and undesirably small samples were obtained.

      Due to the necessity for high weighing accuracy and the
restriction of low tare capacity for the precision electronic
microbalance, greased foil or glass fiber collection substrates
are used with almost all impactors.  Greases have been found to
be unstable at temperatures higher than 400°F, thus glass fiber
substrates were used for this test.

      Backup filters are used to collect the fine particles
which pass the last impactor stage.  One-inch diameter circular
discs are placed under the last spring in the outlet stage of
the impactor.  The filter is protected by a teflon washer and a
second filter disc is placed behind the actual filter to act as
a support.

      The impactors were carefully loaded with the preweighed
collection substrates, assembled, and tightened with pipe
wrenches to make certain that the asbestos gaskets were seated.
Appropriate nozzles were selected for isokinetic sampling.

      The impactors were mounted on probes and placed in the
duct with the nozzles pointed downstream for 45 minutes before
sampling began, to allow them to heat to the gas temperature.
No supplementary heating was used.

      For accurate weighing of collected material, a balance
with a sensitivity of at least 0.05 milligrams is required.
This is especially true for the lower stages of the Brink
Impactor where collection of 0.3 mg. or less is not uncommon.
The balance must also be insensitive to vibration if it is to
be used.  This balance is highly accurate and is insensitive
to vibrations.  A container of Drierite  (anhydrous CaSOn) is
placed in the weighing chamber of the balance to keep moisture
uptake to a minimum during weighing operations and a 500 me.

                              39

-------
Polonium-210  strip  is  mounted in the weighing compartment  for
electrostatic charge neutralization.

       The  balance was  calibrated daily with precision calibra-
tion weights  furnished by Cahn.   Reference and control weights
were also  checked periodically throughout the test series.   The
reference  weights are  standard tare weights while the controls
are impaction substrates which were identical to those actually
used in the impactor runs.

Data Reduction

       Dso cut points are determined by the conditions at which
an impactor was run.  The determination of particle size distri-
butions from the mass  loadings begins with the calculation of
DSQ'S  for each stage,  using an iterative solution of the follow-
ing two equations:


                        V2
1.23 + 0.41 EXP  [(-0.44D5Q)/L x 10-*)]j
      50

 and,

                 2L
     C  = 1  +
             D5Q  x 10-
where    D-- = the  stage  cut  point  (ym),

         y = gas viscosity  (poise),

         D  = stage jet diameter  (cm),
          Lo
         P  = local pressure  at jet  stage  (atm),
          s
         p  = particle density  (gm/cm3),

         Q  = impactor flow rate  (cfm),

         P  = gas pressure at impactor  inlet  (atm),

          C = Cunningham  Correction  Factor,

          L = Gas mean free path  (cm),  and
         K  = Stage calibration constant,  proportional  to

              (50%  efficiency Stokes No.)1/2  for  that  stage.

              The value of Kg for each  stage  is determined  by

              an empirical calibration.
                                40

-------
The viscosity of the gas is calculated using a method presented
by C. R. Wilke in a paper entitled, "A Viscosity Equation for
Gas Mixtures" in the Journal of Chemical Physics , 8J4) , April
1950, p. 517.

      These cut points are calculated by means of a computer
program.  The size parameters used are approximate (Stokes1)
diameter, based on estimated true particle densities, or aero-
dynamic diameters, based on the behavior of unit density spheres.
Aerodynamic diameter is the  diameter of a unit denisty sphere
with the same settling velocity as the particle in question.
The aerodynamic diameter is calculated by giving p  the value
of 1.0 gm/cm3 in the D5o  formula.                 p

      The data are presented on a cumulative basis by summing
the mass on all the collection stages and backup filter, and
plotting the fraction of the mass below a given size  versus
size.  This is frequently done on special log-probability
paper.  This paper is especially convenient for log normal dis-
tributions, but semi-log paper may be preferable for interpreta-
tion, especially if the distribution is not log normal.  In
general, cumulative distributions are more difficult to inter-
pret than differential plots.  The abscissa is the logarithm of
the particle diameter, and the ordinate is the percentage
smaller than this size.  The value of the ordinate at a given
(D50)n  is
                                        E
       Percent less than stated size = — ^ - x 100%

                                        E    dMt
                                       t = o

where t = o corresponds to the filter, and
      t = N corresponds to the coarsest jet or cyclone.

      In addition, the data are presented as differential parti-
cle size distributions.  For this purpose it is assumed that all
of the mass caught upon an impaction stage consists of material
having aerodynamic diameters equal to, or greater than the Dso
for that stage, and less than the Dso for the next higher
stage.  For the first stage (or cyclone) , it is assumed that all
the material caught has aerodynamic diameters greater than, or
equal to the Dso for that stage (or cyclone) , but less than or
equal to the size of the largest particle present.  The latter
size is determined by microscopic examination of the material
caught on the stage.

      Because the intervals between the stage Dso's are usually
logarithmically related, and to minimize scaling problems, the
differential partice size distributions are plotted on log-log


                               41

-------
 or semi-log paper with

                               dM
                            a  (log D)

 as the ordinate and Dgeo as the abscissa.  (Daeo is the geo-
 metric mean of DI and D2.)   The mass on stagey"n" is designated
 by dMn.  The d (log D) associated with dMn is log D50)n+l-log
 (Dso )n.  The total mass having diameters between (D50)n  is equal
 to the area under the curve
         n

 Mass = / y
t-m  log (D^)	-log  (Deft),' L"=  <"50't+i ""  ^SO^]
or

            D
 for a continuum.

       The procedure outlined above describes the construction of
 a histogram.   A smooth curve is drawn through the points,
 yielding an approximation to the real particle size distribution.
 Such a curve is needed to calculate fractional efficiencies of
 control devices if the Dso's  differ between inlet and outlet
 measurements.  The accuracy of the approximation is limited by
 the number of points, and by the basic inaccuracy of neglecting
 the non-ideal behavior of the impactors, especially the non-
 ideal overlapping efficiencies for adjacent stages.

       Dividing dM/dlogD of an outlet run at a particle size by
 the dM/dlogD from its comparable inlet run at the same size
 gives the fractional penetration through the control device of
 that size particle.  The fractional penetration subtracted from
 unity is the fractional efficiency of the control device.

 DATA

       Table  9  shows the weight changes measured for the blank
 Brink impactor runs.  The glass fiber substrate material used
 was Reeve Angel 934AH.  Our experience with this material  has
 shown that weight changes due to flue gas gas phase reactions
 are usually small, especially when "preconditioned" by exposure
 to flue gas prior to an actual run.  Another pre-conditioning

                               42

-------
          TABLE 9.   BRINK IMPACTOR  BLANK RUNS*
    SUBSTRATE WEIGHT CHANGE FOR EXPOSURE TO FLUE  GAS
Run Number 7
Substrate Set Al
Type of H2SCU
Conditioning wash
Run Time
Run Date
SO

SI
S2
*> S3
CO
S4
85
S6
SF
SF1
SO - S6
SF - SF1
SO - SF1
15 min
6/30
-0.07 mg
change
-0.09
-0.05
+0.01

-0.09
-0.19
+0.02
-0.06
-0.27
x=-0.01
x=-0.12
x=-0.04
5
A2
. H2SO,,
wash
15 min
6/29
+0.01 mg
change
+0.02
+0.08
+ 0.11

+0.01
+0.04
+0.01
-0.06
-0.09
0-0.08
0=0.10
0=0.09
8
A3
None
30 min
6/30
+0.04 mg
change
+0.05
+0.04
+0.03

+0.02
+0.01
Lost
Lost
Lost
x=0.05
x=0.16
x=0.06
6
A4
None
15 min
6/29
+ 0.07mg
change
+ 0.10
+0.07
+0.06

+ 0.06
+ 0.03
+0.03
+ 0.15
+0.17
0=0.02
0=0.01
0=0.05
13
A5
In-situ
15 min
6/30
-0.01 mg
change
+0.00
-0.01
+ 0.01

-0.01
+0.00
-0.03
-0.11
-0.08
x=-0.02
x=-0.13
x=-0.04
16
A6
In-situ
15 min
7/1
-0.03 mg
change
-0.02
-0.03
-0.02

-0.04
-0.02
-0.05
-0.23
-0.11
0=0.02
0=0.07
0=0.06
4
Jll
In situ
60 min
7/10
+0.06 mg
change
-0.07
-0.02
-0.05

-0.01
-0.03
-0.03
-0.17
-0.06
x=-0.02 0=0.04
x=-0.12 o=0.08
x=-0.04 0=0.06
*Reeve Angel 934AH substrate material.

-------
 agent which could offer promise is sulfuric acid, since flue gas
 induced weight gains are found to be sulfate compounds.2  Sub-
 strate sets Al and A2 were washed in sulfuric acid followed by
 a thorough rinse.  The weight changes recorded in Table 9 are
 listed stage by stage, from "stage zero", to SF1 , which is back-
 up filter number two.  Averages, and standard deviations about
 those averages, are given for stages zero through backup filter
 two.   Impactor substrates for stages zero through six typically
 weigh 14 milligrams apiece and backup filters normally average
 about 32 milligrams apiece.

 Outline of Data Reduction Procedures

1. Calculate Dso's.

2. Convert Stage Weights To MG/ACM or MG/DSCM.
                                        n M
3. Plot Cumulative Size Distribution.   E ^ vs.  (D5o) t+^
                                       t=o

4. Plot Cumulative % Size Distribution. %< D5o vs. Dso
5. Plot Differential Size Distribution.  (dM/d log D)n vs./Di-Di+1

                          dM/d log D, Outlet
6. Calculate Penetration.
                          dM/d log D, Inlet
       Based on the results of these tests, unconditioned sub-
 strates were used for all the impactor tests on July 9 and 10.

       Table 10 through 27 contain computer reduced data for all
 inlet and outlet impactor runs on July 9 and 10.  The first line
 of the printout gives the run location, the run number, the run
 date, the start time, the port number, and pantleg designation
 as indicated below.

      1-1
 Location:

 I-Inlet

 0-Outlet
  07-09-76

      I
    Date

Run Number
0720


Start

 Time
   4
West
   /          f
 Port     Pantleg
Number  Designation
       The data are reduced assuming particle densities of 1.0
 (aerodynamic) and 3.58gm/cm3, and complete printouts are includ-
 ed  for  each assumed density.
                               44

-------
                                                          TABLE  10.
     1-1   07-09.76  0720   ttWEST
  IMPACTOR FLOWRATE  » 0,029 ACFM               IMPACTOR  TEMPERATURE o   tso.o  F  s  343,3  c               SAMPLING  DURATION  =   50,00  MN
  IMPACTOR PRESSURE  DROP  • 0,6 IN,  OF  HG       STACK  TEMPERATURE  •   65o,o  F  • 343,3  c
  ASSUMED PARTICLE DENSITY « 3,58 GM/CU.CM,      STACK PRESSURE  *  26,15  IN, OF HG     MAX,  PARTICLE  DIAMETER  •  100,0  MICROMETERS
  GAS COMPOSITION (PERCENT)           C02 •   6.40          CO  =  0,00            N2 • 71,36          02 *   5,50           H20  •  15,00
  CALC,  MASS LOADING • 6.0J46E.01 GR/ACF             1.5607E+00 OR/DNtF              1.3609E+05  MG/ACM              3,57102
  CUM, (GR/DNCF) SMALLER  THAN 050         2.4SE-01   1.99E-01  1.77E-01   1.45E-01   1.52E-01  1.20E-01   1.09E-01   7.58E-02
  GEO, MEAN DIA, (MICROMETERS)            3.24E+01   8,35E*00  4.76E+00   2.48E+00   l,62EtOO  1.07E+00   fc,52E«01   i,85F-01   1.9SE-01
  DM/DLOGD (MG/DNCM)                      5.08E+03   5,11E»02  1,73E*02   2.67E+02   3,33E»02  9,74E
-------
                                                             TABLE 11.
    I»t  07-09.76  0720  4WE8T
 IMPACTOR HOWRATE » 0,029 ACFM               IMPACTOR TEMPERATURE  »  tso.o f = 343,3 c              SAMPLING DURATION «   50,00 HIN
 IHPAGTOR PRESSURE DROP • 0,6 IN, OF HG       STACK TEMPERATURE •   650,0 F « 343.3 C
 ASSUMED PARTICLE DENSITY •  i.OO GM/CU.CM.     STACK PRESSURE * 28,15 IN, OF HO     MAX, PARTICLE DIAMETER • 180,3 MICROMETERS
 5*8 COMPOSITION  (PERCENT)           COS *  6,00          CO •  0,00           N2 i 71,36          02 »  5,50           H20 « 15.00
 CALC, MASS  LOADING  •  6.0346E.01 GR/ACF             1.S607E+00 GR/DNCF             1.3809E+03 HG/ACH             3.5714E+03 MG/ONCM
 IMPACTOR STAGE                           CVC        SO        Si        12        83        84        85        S6     FILTER
 STAGE INDEX NUMBER                         i23«S6?*9
 050  (MICROMETERS)                       19,63      12,75      6,60      3,97      2,«t       1,61      1,17      0,66
 MASS  (MILLIGRAMS)                       28,72      0,96      0,48      0,70      0,29       0,25      0,24      0,73      1,65
 MG/DNCM/8TAGE                           3,01E*03  i,01E+02  5,0«E*01  T.J5E+01  3,OttE*01   2,62E*01  2,52E*01  T.66E+01  1,73C*02
 CUM,  PERCENT OF  MASS  SMALLER THAN  oso   is,SB      12,76      11,35      9,29      6tnu       7,71      7,oo      a,86
 CUM.  (MG/ACM)  SMALLER THAN  050          2.15E+02  1,76E*02  1,97E*02  1,28E*02  1.17E+02   1.06Ef02  9,67E«01  6.70E«01
 CUM.  (MG/DNCM)  SMALLER THAN 050         5,57E*02  4.56E+02  4.05E+02  3,J2E*02  3,01E*02   2,73E*02  2.50E+02  1.73E+02
 CUM,  (GR/ACF)  SMALLER THAN  OSO          9,«OE-02  7.70E-02  6.85E-02  5.61E-02  5.09E-03   4.65E-02  4,22E»02  2,93E*02
 CUM.  (GR/DNCF)  SMALLER THAN 050         2.43E-01  1.99E-01  1.77E-01  1.45E-01  1.32E-01   1.20E-01  1,09E»01  7,58E»02
 GEO,  MfAN  CIA,  (MICROMETERS)            6,13E»01  1,59E+01  9,17E»00  U,85E*00  3,23B*00   2,19E+00  1,39E*00  8,78E«01  «,65E»OJ
 OM/DLOGD (MG/DNCM)                      3,08E*03  5.26E+02  1.76E+02  2.75E+02  3,U9E»02   1.05E+02  1,7«E»02  S,0«E»02  5,75E»0?
  DN/DLOGD (NQ,  PARTICLES/DNCM)           2.36E+07  2.50E+OB  U,35E»08  U.60E+09  1.98E+10   1.91E+10  1.25E+U  8.58E+11  1.09E+13


NORMAL (ENGINEERING  STANDARD) CONDITIONS  ARE 21 OEG C AND  760MH HG.

-------
                                                              TABLE 12.
     1*2 07»09«76  OTOB  JNE8T
  IHPACTOR FLOWRATE • o,056 ACFM               IMPACTOR TEMPERATURE *  650,o F « 343,3 c              SAMPLING DURATION •  20,00 HIN
  IMPACTOR PRESSURE DROP • 2,2 IN, OF HC       STACK TEMPERATURE •  6so.o F * 343,3 c
  ASSUMED PARTICLE DENSITY • 3,98 GM/CU.CM.     STACK PRESSURE • 26,80 IN, OF HG     MAX, PARTICLE DIAMETER • 100,0 MICROMETERS
  CAS COMPOSITION (PERCENT)           C02 •  6.140          CO •  0,00           N2 o 71,36          02 •  5,50           H20 » IS,00
  CALC, MASS LOADING • l,»fll5En01 GR/ACF             S.0121E-01 GR/DNCF             4.U427E+02 MG/ACM             1,1«69E»03 MG/DNCM
  IMPACTOR STAGE                           CYC        SO        Si        82        83        Stt        35        86     FILTER
  STAGE INDEX NUMBER                         12S056789
  050 (MICROMETERS)                       7,50      «,7«      2,00      1,25      1,01      0,52      0,3fl      0,15
  MASS (MILLIGRAMS)                      11,65      0,07      0,05      0,02      0.06      0,16      0.3U      0,58      1,16
  MG/DNCM/8TAGE                           9,«8E*08  5,70t*00  0,07E*00  1,63E*00  a,e6E+00  1,30E+01  2,77E»01  «,72E+01   9.UUE+01
  CUM, PERCENT or MASS SMALLER THAN 050  17,32     u.si     i6,ur     16,33     is.fo     10,77     12,35      9,20
  CUM, (MG/ACM) SMALLER THAN D50          7,70Et01  7,«BE*01  7.32E*01  7.25E+01  7.07E»01  6.56E+01  5,«9E»01  3,66Ef01
  CUM, (HG/DNCM) SMALLER THAN OSO         1,99E+02  1,93E*02  1.8?E*02  I,87E*02  1.82E+02  1,6«E+02  I,02  1,60E*02
  CUM, (GR/DNCF) SMALLER THAN DSO         8.68E.02  8,«3E»02  8.26E-02  8,1SE«02  7,«7E>02  7.00E-02  6,m-02  4,13E>02
  GEO, MEAN DIA, (MICROMETERS)            2.75E+01  5.98E+00  I.37E+00  1.73E+00  1,12E*00  7.J2E-01  4,21E<01  2,25E«01   1.0«E-01
  DM/DLOGD (HG/DNCM)                      S.05E+02  2,62E*01  1.S8E+01  5.76E+00  5.1JE+01  4,53Et01  1,53E*02  l.IOE+02   3.1UF+02
  DN/DLOGD (NO. PARTIC.LES/DNCM)           2,18E*07  7.05E+07  1.91E*OB  5,90EtOS  1.9UE+10  6,U3E*10  1.09E+12  6.06E+1J   l,U7EilU


NORMAL (ENGINEERING STANDARD) CONDITIONS ARE 21 DEC C AND 760MM MG,

-------
                                                              TABLE  13.
    J«2 OT-09.76   0700   SWEST
 IMPACTOR FLONRATE  •  0,056  ACFM                IMPACTOR  TEMPERATURE  •  650,0  F  «  343,3  C               SAMPLING  DURATION  *   20,00  HIN
 IHPACTOR PRESSURE  DROP  « 2,2  IN,  OF  HG        STACK  TEMPERATURE  •   650,0  P « 3«3,3  C
 ASSUMED PARTICLE  DENSITY • 1,00 GM/CU.CM,      STACK  PRESSURE =  28,20  IN,  OF HG      MAX,  PARTICLE  DIAMETER  •  189,2  MICROMETERS
 CAS  COMPOSITION  (PERCENT)            COB  •   6,00           CO  «  0,00          Ng • 71,36          02 »   5,50           M20  •  15,00
 CALC, MASS  LOADING • 1.941SE.01 CR/ACF              5.0121E-01 GR/DNCF             4,44'87E*02  MG/ACM              1.1«69E»OS  MG/ONCM
 IMPACTOR STAGE                           CVC         SO       81         82         8}        81        SS        86    FILTER
 STAGE INDEX NUMBER                         123056789
 050  (MICROMETERS)                       14,27      9,1J      a.70       2,52      2,05       1,13       0,79      0.40
 MASS (MILLIGRAMS)                       11,65      0,07      0.05       0,02      0,06       0,16       O.Jtt      0,58      1,16
 MG/ONCM/STAGE                            9,4SEt02  5,70E*00   0.07E*00   1.63E + 00  U.BBE + 00  1,JOE*01   2,77E*Ol   (|,72E«01   9,«ilE»01
 CUM, PERCENT OP  MASS SMALLER  THAN D50   17,32      16,63     16.«7      16,33      15,90      14,77      12,35      8.2U
 CUM, (MG/ACM)  SMALLER THAN D50           7.70E+01  7,«BE*01   7,32E«01   T.25E»01  7.07E*01  6,56E*01   5,49E«01   3.66E+01
 CUM, (MG/DNCM)  SMALLER  THAN 050          1,99E»02  1.93E+02   1.89E+02   1.87E*02  1.82E+02  1.69E+02   1,42E«02   9,«5Et01
 CUM, (OR/^CF)  SMALLER THAN 050           3.36E-02  3.Z7E-02   3.80E-02   5.17E-02  3.09E-92  2.S7E-02   2,«OE-02   1.60E-02
 CUM, (GR/DNCF)  SMALLER  THAN 050          6,68E-02  B.U3E-02   6.26EP02   B.18E-02  7,97E«02  7.40E-02   6,19E-02   U.13E-02
  GEO, MEAN  DIA,  (MICROMETERS)             5,20E*01  l,iaE»01   6.55E+00   3.04E+00  2.27E+00  1.52E+00   9,a6E-Ol   5.62E-01   2.82E-01
  DM/OLOGD  (MG/DNCM)                      8.05E+02  2.94E+01   1.41E+01   6,02E*00  5.UBE+OI  S,02E«01   l,SOEt02   1,59E»02   3,14E*02
  DN/DLOGD  (NO,  PART1CLES/ONCM)           1,15E*07  3,77E*07   9,60E*07   2,82E*08  8.91E+09  2.72E+10   «,05E+11   1,70E»12   2,66E*13


NORMAL (ENGINEERING STANDARD) CONDITIONS  ARE 21 DEC C  AND 760HM HG,

-------
                                                           TABLE 14.
     1-3 07.09.T6   1135  3EAST
  •IMPACTOR FLOWRATE = 0.029 ACPM               IHPACTOR TEMPERATURE «   625,o f •  129.11 c              SAMPLING  DURATION  «   30,00 n*
  IMPACTOR PRESSURE DROP • 0.6 IN.  Of HG       STACK TEMPERATURE •  625,0  f  ' 329.4 C
  ASSUMED PARTICLE DENSITY • 5,56 GM/CU.CM',      STACK PRESSURE i 26,20 IN,  OP HG      MAX,  PARTICLE  DIAMETER  •  100.0  MICROMETERS
  GAS COMPOSITION (PERCENT)           COB •   6.UO          CO •  0.00            N2 . 71,36          02 >   5.50           H20  c  15.00
  CALC,  MASS LOADING • 4.J317E.01 GR/ACF             1.0931E*00 GR/ONCF             9.9124E+02 MG/ACM              2,501«E+03  HG/DNCM
  IMPACTOR STAGE                           cvc        so        si        sz        ss        34         ss        86    FILTER
  STAGE  INDEX NUMBER                         123456789
  D50 (HICROHETCRS)                      10.39      6.60      3,36      1.79      1,45      0.76       0,50      0,27
  MASS (MILLIGRAMS)                      19,24      0,24      0.36      0,49      0.29      1.54       0,66      0,56      1,02
  MG/DNCM/STAGE                           1.97E+03  2,46E*01   J,89E*01  5,02E»01   2.9TE401  1,5SE«02  6,76E*01   5,74E*01   1.04Et02
  CUM. PERCENT OF MASS SMALLER THAN DSO  21,22     20,23     is.66     i6,*7     is,«e      9,16       6,48      q.is
  CUM, (MG/ACM) SMALLER THAN DSO          2,}OE*02  2,01E*02   1,85E*02  1.65E+02   1,53E*02  9.JOE+01  6,42E*Ol   U.15E+01
  CUM, (MG/DNCM) SMALLER THAN DSO         5,31E^02  5,06E*02   4,67E»02  4.17E+02   J.87E+02  2.30E»02  1,62E«02   1,05E*02
  CUM, (GR/ACF) SMALLER THAN 050          9,19E*02  8.76E-02   8.09E-02  7.22E.02   6,718-02  3.96E.02  2.60E-02   1.81E-02
  CUM, (GR/DNCF) SMALLER THAN DSO         2.32E-01  2.21E.01   2.04E-01  1.82E-01   1,69E>01  l.OOE-01  7.08E-02   1.57E-02
  GEO. MEAN DIA, (MICROMETERS)            3.22E«oi  S.ZBE+OO   «,72E+oo  2,«6E+oo   i,6]E*oo  i.o7E*oo  6,soE>oi   i.eaE-oi   i,93E-oi
  DM/OLOGD (MG/DNCM)                      J.OOE+OS  I.ESE+OS   i,34E
-------
                                                                 TABLE  15.
         I"3  07.01.76    H3S   3EAST
      IMPACTOR  FlONRATE  *  0,029  ACFM                IMPACTOR TEMPERATURE •   625,0 f • 329.8 C               SAMPLING DURATION •  30,00 HIM
      IMP«TtJR  PRESSURE  DROP  • 0,6  IN,  OP  HO        STACK  TEMPERATURE  •   629.0 F  • 329,0 C
      ASSUMED PARTICLE DENSITY • i.OO  GM/CU.CM.      STACK PRESSURE  •  28,20 IN,  OF HG     MAX.  PARTICLE  DIAMETER • 189,2 MICROMETERS
      6A8 COMPOSITION  (PERCENT)            C02 .   6.«0          CO .  0,00            N2 . 71.36          02 •  5,50           H20 • 15.00
      CAUC,  MASS  LOADING • Jl.331TE.01  OR/ACF              1.0931E*00 GR/DNCF              9,912«E*02  MG/ACM             2,501
-------
                                                             TABLE  16.
     1.4 OT.09.Tfc   1200  4EAST
  IMPACTOR FLONRATE = o,o«« »CFM               IMPACTOR TEMPERATURE •  625,0 t « 329,4 c              SAMPLING DURATION «  30,00 KIN
  IMPACTOH PRESSURE DROP • i.« IN, OF MS       S-TACK TEHPERATURE «  435,0 f  » 329,4 c
  ASSUMED PARTICLE DENSITY " 3,58 GM/CU.CM,     STACK PRESSURE B 28,20 IN, OF HG     MAX, PARTICLE. DIAMETER » 100,0 MICROMETERS
  CAS COMPOSITION (PERCENT)           C02 f  6.00          CO »  0,00           N2 • 71,1*          02 •  5,50           H20  «  15,00
  CALC, MASS LOADING « 4.456TE.01 GR/ACF             !,12a6E02  2,89E>02  1.U2E.02
  CUM, (GR/DNCF) SMALLER THAN DSO         3,?9E>01  2,71E.Q1  1.67E.01  1.12E.01  1.11E.01  8.80E.02  7.29E.02  1.58E.-02
  GEO, MEAN DIA, (MICROMETERS)            2,90E*Ot  6,7lE*00  S.SOEtOO  1,97E*00  1,28E*00  8,3«E"01  4.96E.01  2.78E-01   1,3«E-01
  DM/DLOGO (MG/DNCM)                      1,59E*OS  1,21E*03  6,78E»02  3.67E+02  7,59Ef02  1.86E+02  2,01Et02  2.57E+02   2,71E»02
  ON/OLOGO (NO, PARTICLE8/DNCMJ           3,«6E*OT  2,15E*09  6,59E*0«  2,58E*10  1,93E»H  1.T2E+11  S,76E*11  fc.S7E»12   5,96E»13
NORMAL (ENGINEERING STANDARD) CONDITIONS ARE 21 DEC C AND 760MM HG,

-------
                                                                TABLE 17.
       I-U 07.09.76   1200  «EAST
    IMPACTOR FLDNRATE • o,o«« ACFM               IMPACTOR TEMPERATURE  «  625,o F » 329.4 c              SAMPLING DURATION  .   jo.oo  HIM
    IMPACTQR PRESSURE DROP • l.« IN, Of HG       STACK TEMPERATURE •   625,0 F « 329,4 C
    ASSUMED PARTICLE DENSITY «  1.00 CM/CU.CM.     STACK PRESSURE • 28,20 IN, OF HG     MAX, PARTICLE DIAMETER * 189,2 MICROMETERS
    CAS COMPOSITION  (PERCENT)           C02 *  6.40          CO o  0,00           N2 n 71,J6          02 •  5,50           H20 *  15.00
    CALC, MASS LOADING • 4.0S67E.01 GR/ACf             1.1206E*00 6R/DNCF             1.019BE*03 MG/ACM             2.5735E*OJ MG/DNCM
    IMPACTOR STAGE                           CYC        80        81        82        S3        84        85        86     FILTER
    STAGE INDEX NUMBER                         123056789
    DSO  (MICROMETERS)                       15,«T      10.24      5.26      3,84      2,32       1.29      0.91      0,49
    MASS  (MILLIGRAMS)                       25,26      I,i9      2,95      1,52      1,05       0,77      0,51      1,26      1,21
01  MG/DNCM/8TAGE                           1,71E»03  2,42E*OZ  1,99E*02  1.03E+02  7.09E+01   5.20E+01  3.44E+01  8,51E*01  8,17E»01
to
    CUM,  PERCENT OF  MASS SMALLER THAN  DSO   33,74      20,32      I6,se     12,60      9,84       7,82      6,48      5,ie
    CUM,  (MB/ACM) SMALLER  THAN  050          3,44E*02  2,08E*02  1.69E+02  1.2BE+02  1,OOE»02   7.98E+01  6,61E*01  J,24E*01
    CUM,  (MG/DNCM)  SMALLER THAN 050         8.68E+02  6,26E»02  4.27E402  3,20E*02  2,53E«02   2,01E*62  1,67E*02  8,18E»01
    CUM,  (GR/ACF) SMALLER  THAN  050          1.50E-01  1.08E-01  7.39E.02  5.61E-02  U.39E-02   3.49E-OZ  2.89E.02  1.42E-02
    CUM,  (GR/DNCF)  SMALLER THAN 050         3.79E-01  2.74E-01  1.87E-01  1.42E-01  l.HE-01   8.80E-02  7.29E-02  3.58E-02
    GEO,  MEAN  OIA,  (MICROMETERS)            5,50E+01  J,28E»Ol  T,35E*00  3,88E*00  2,57E*00   1.73E+00  1.09E+00  6.67E.01  3.44E-01
    DM/DLOGD  (MG/DNCM)                      1.59E+03  1.26E+03  6.93E»02  3.82E+02  8.03E+02   2.04E+02  2,30E*02  3,11E*02  2.71E+02
    DN/DLOGD  (NO,  PARTICLES/DNCM)           1.83E+07  1.15E+09  3.33E+09  1,25E*10  
-------
                                                            TABLE  18.
     1-3  7.10*76  0600  3EA8T
  IMPACTOR FLOWRATE » 0,018 ACFM               IHPACTOR TEMPERATURE »  615,0 F  P 323,9 C               SAMPLING  DURATION  >   30,00  MIS
  IMPACTOR PRESSURE DROP « 1,1 IN, OF HC       STACK TEMPERATURE »  615,0 F  » 323.9 C
  ASSUMED PARTICLE DENSITY • 3,56 GM/CU.CM,     STACK PRESSURE • 28,28  IN, OF H6     MAX,  PARTICLE  DIAMETER  *  100.0  MICROMETERS
  6A8 COMPOSITION (PERCENT)           COS t  6.40          CO  *  9,00           N2 • 71,36          02 a   5,50           H20 •  15.00
  CALC, MASS LOADING • 1.3402E.01 GR/ACF             3.341ZE-01 OR/DNCF             3.0668E+02  MG/ACM              7,6458E*02 MG/DNCM
  IMPACTOR STAGE                           CYC        SO        81        32        83       84        85        86    FILTER
  STAGE INDEX NUMBER                         1234S6T89
  D90 (MICROMETERS)                       9,0!      5,73      2,92      1,50      1,29      0,66       0,45      0,22
  MASS (MILLIGRAMS)                       4,55      0.25      0,35      0,36      0,29      0,30       1,18      1,06      1,56
  MG/DNCM/BTAGE                           J.51E+OZ  1.93E+01   2.70E*01   2,78E»01  2.24E*01  Z.32E+01  9.HE + 01   8.10E+01  1.20E+0?
  CUM, PERCENT OF MASS SMALLER THAN 050  54,05     51,52     47,98     44,35     41,«2     38,39      26,47     15,76
  CUM, (MG/ACM) SMALLER THAN D50          1,66E+02  1.58E+02   1.U7E+02   1.36E+02  1.27E*02  1.18E+02  6,I2E»01   U.83E+01
  CUM, (MG/DNCM) SMALLER THAN 050         4,13E+02  3.94E+02   J.67E+02   3,39E*02  3.17E+02  2.94E+02  2,02E*02   1.21E402
  CUM, (GR/ACF) SMALLER THAN 050          7,24P»02  6.90E-02   6.U3E-02   5,9aE-02  5.55E.02  5.14E-02  3.55E-02   2.11E-02
  CUM, (GR/DNCF) SMALLER THAN 050         1,81E>01  1.72E-01   1.60E-01   1,4BE»01  1.J8E.01  1,2BE«01  8,6«E>02   5.27E-02
  CEO, MEAN OIA, (MICROMETERS)          "  S,OIE»OI  7,aoE+oo   «.o9E+oo   a.i2E+oo  i.J9E+oo  9,o9E»oi  s,u7E>oi   J.IUE-OI  I.SUE.OI
  DM/DLOGD (MG/DNCM)                      J.J7E+02  9.73E+01   9.2«E*01   1,OOE«02  2,«2E+02  8.44E+01  5,45E*02   2.59E+02  4,OOE»02
  DN/DLOGD (NQ, PARTlCLES/DNCM)           6.60E+06  1,39E»08   7.JOE+OS   S.59E409  U.B5E+10  6,OOE»10  1.78E+12   4,U9E«12  5.8JE+13


NORMAL (ENGINEERING STANDARD) CONDITIONS ARE 21 DEC C AND 760MM HG.

-------
                                                            TABLE  19.
    1-5  T.10.76  0640  3EAST

 IMPACTOR FLOWRATE • 0.038 ACFM                IMPACTOR  TEMPERATURE •   619,0  F  "  323.9  C               SAMPLING  DURATION  x   30,00  HIM

 IMPACTOR PRESSURE DROP a  1,1  IN, OF HG        STACK  TEMPERATURE  •  6J5.0  F " 323,<>  C

 ASSUMED PARTICLE DENSITY  >  1.00 GM/CU.CM,      STACK PRESSURE  •  28,26  IN, OF HC     MAX,  PARTICLE  DIAMETER  «  189,2  MICROMETERS

 0A9 COMPOSITION  (PERCENT)           C02  «   6,40           CO •  0,00           N2 • 71,16          02  •   5,50           H20  «  IS,00

 CALC, MASS LOADING •  i,S«C2E«01 GR/ACF              S,3«12E»01 6R/DNCF              3,0668E*02  HG/ACH              7,602  5,1«E«02   3.5SE-02  2.11E-02

 CUN,  (6R/DNCF)  SMALLER THAN 050          1,81E»01   1.72E-01  l,60E«Sl   1.1BE-01  1.38E-01  1.28E-01   8,8«E-02  5.27E-02

 GEO,  MEAN  DIA,  (MICROMETERS)             5,69E*01   l.JTE+01  7,90E»00   4.17E+00  2,77E*00  1.87E+00   l,lflE*00  7.35E-01  3,8aE«01

 DM/OLOGO  (MG/ONCMJ                       3,37E+02   1,OOE+02  9,a2E*01   1,0«E+02  2.55E+02  9,15E»01   6,19E*02  3,ilE*02  a,OOE*02

 ON/DLOGD  (NO,  PARTICLE3/DNC")           3,«9E*06   7,«2E+07  3.65E»06   2.73E+09  2,29E*10  2,6?E»10   7,20E»H  I.«9E»|2  I,356*13




NORMAL (FNG1NFERING  STANDARD) CONDITIONS  ARE SI DEG C AND  760MM HG,

-------
                                                               TABLE  20.
     1.7 07-01-76   1000  SNEST
  IHPACTOR FLOWRATE • o.osa ACFM               IMPACTOR TEMPERATURE »  tis.o f  * 333.9 c              SAMPLING DURATION a  20.00  HIM
  IMPACTOR PRESSURE DROP • 1.1 IN. OP HG       STACK TEMPERATURE •  6i5,o f « 523.9 c
  ASSUMED PARTICLE DENSITY » 3.58 GM/CU.CM.     STACK PRESSURE • 26,28 IN. OF HO     MAX. PARTICLE DIAMETER • 100,0 MICROMETERS
  GAS COMPOSITION (PERCENT)           C02 •  6,00          CO «  0,00           N2 • 71,1*          02 *  5.50           H20 «  IS,00
  CALC, MASS LOADING • 9.0767E-08 GR/ACF             2.2629E-01 GR/ONCF             2.0771E+02 MG/ACH             5,1783E*02 MG/DNCM
  IMPACTOR STAGE                           CYC        so        91        32        33        34        35        36     FILTER
  STAGE INDEX NUMBER                         123056789
  050 (MICROMETERS)                       9,05      3,73      2,*2      1,54      1,25      0,66      0,45      0,22
  MASS (MILLIGRAMS)                       0,00      0,27      0,49      0,85      0,40      0,97      0,4b      0.65      0,40
  MG/DNCM/STAGE                           O.OOE-01  3.13E+01  5.68E+01  9,62E*01  4,63E*01  1,12E»02  5,33Et01  7.53E+01   4.63E+01
  CUM, PERCENT OF MASS SMALLER THAN oso 100,00     93,96     83.oo     64.43     55,49     33.79     23,49      8.95
  CUM. (MG/ACM) SMALLER THAN D50          2.06E+02  1,95E»02  !.72E*02  1,34E«02  1.1SE*02  7,02Et01  4,88E401  l.«6E+01
  CUM, (MG/DNCM) SMALLER THAN 050         5.18E+02  U,87E»02  4,30E«02  3,34E*02  2,87E^02  1,75E«02  1,22E*02  U,64E»01
  CUM, (GR/ACF) SMALLER THAN 050          9,OSE»02  8,53E«02  7.53E-02  5,851-02  5,04E»02  3.07E.02  2,13E>02  8,13E>03
  CUM, (GR/DNCF) SMALLER THAN D50         2,26E>01  2.13E-01  1.88E.01  I,46E>01  1.26E-01  7.6SE-02  5,32E>02  2.0JE-02
  GEO, MEAN DIA, (MICROMETERS)            3,01E»01  7,20E»00  4,09E*00  2,12E+00  1,39E+00  9,09E-Ot  5.47E-01  i,14E«01   J,SUE.01
  DM/DLOGD (MG/DNCM)                      O.OOE-Ol  1,58E*02  1.94E*02  3.47E+02  5,01E»02  «,0«E+02  3,19E*02  2,39Et02   1.54E+02
  DN/DLOGD (NO, PARTICLES/DNCM)           O.OOE-01  2,25E»08  1.51E+09  1.93E+10  l.OOE+11  2.91E+11  1,04E>12  4,13E+12   2,24Ei|3


NORMAL (ENGINEERING STANDARD) CONDITIONS ARE 21 DEC C AND 760MM HS,

-------
                                                              TABLE  21.
    1.7 07«01«7*    1000   SNE8T
 IMPACTOR FLOHRATE  •  0,058  ACFM                IMPACTOR  TEMPERATURE  -   615,0  f  *  525,9 C               SAMPLING DURATION .  20,00 MIN
 IMPACTOR PRESSURE  DROP  • 1,1  IN,  OF  HG        STACK  TEMPERATURE  •  615,0  P  • 523,9 C
 ASSUMED PARTICLE DENSITY . 1.00 GM/CU.CM,      STACK PRESSURE  .  28,28  IN, Of HC      MAX.  PARTICLE DIAMETER »  189,2 MICROMETERS
 CAS  COMPOSITION  (PERCENT)            C02  •   6,40           CO  •  0,00            N2 . 71,36          02 «  5,50           H20 •  15.00
 CAUC,  MASS  LOADING . 9.0767E-02 GR/ACF              2.2629E-01 OR/DNCF             2.0T71E*02 MG/ACM             5,1785E*02 MG/DNCM
 IMPACTOR STAGE                           CYC         SO       81        82         »5        84        35        36     FILTER
 8TA6E  INDEX NUMBER                         1          2         3        4          5         6         7         8         «
 D50  (MICROMETERS)                       lT.12      10,M      5.68      3,06       2.50      l.«0      1,00      0,5a
 MASS (MILLIGRAMS)                        0,00       0,27      0,49      0,85       O.«0      0.97      0,06      0.65      O.UO
 MG/DNCM/STAGE                            O.OOE-01   3.13E+01   5.6BE*01   «».62E*01   «,65E*Ol  1.1ZE*02  5,33E*01  7.53E*01   «,63F*01
 CUH, PERCENT OF  MASS SMALLER  THAN DSO 100,00      95,96     ss.oo     6a,«3      55,«9     33,79     23,09      8.95
 CUM, (MG/ACM)  SMALLER TMAN 050           2,08E*02   l,95E»oa   1,72E*OZ   1.30E+02   1.15E*02  7,02E»01  «,88E»01  1.86E»01
 CUM. (M8/DNCM)  SMALLER THAN 050          5,18E»02   «,87E»02   4.30E*02   3,3«B»02   2,87E»02  l,75f»02  1,22E*02  a,6«E*01
     . (GRAACF)  SMALLER THAN 050           9.08E.02   e,53E.02   7.55E-02   5,»SE-OI   5.04E.02  3.07E.02  2.15E-02  8.13E-03
     , (GR/DNCF)  SMALLER THAN 050          2.26E-01   2.13E-01   1.88E-01   1.16E.01   1.26E.01  7.65E-02  5.32E-02  2.03E-02
  GEO.. ME-ANDIA.  (MICROMETERS)             5,69E*01   1.37E+01   7.90E+00   a,17E*00   2.77E»00  1.87E»00  1,18E*00  7.35E-01   3,8ttE-01
  DM/DLOGD  (MG/DNCM)                      O.OOE-01   1.63E+02   1.9BE*02   3.59E+02   5.28E*02  a,««E+02  3.62E+02  2.86E*02   1.5«E*02
  DN/DLOGD ,(NO.  PARTICLES/DNCM)           O.OOE-01   1.20E*08   7.66E»06   9,4
-------
      0-1B  07-09.76  0720  1PORT
  IMPACTOR FLOWRATE * 0.073 ACFM
  1MPACTOR PRESSURE DROP » 3,6 IN, OF H6
  ASSUMED PARTICLE DENSITY • 3,56 GM/CU.Ch.
  CAS COMPOSITION (PERCENT)           C02 •
  CALC, MASS LOADING • I.0320E-02 GR/ACF
  IHPACTOR STAGE
  STAGE INDEX NUMBER
  D50 (MICROMETERS)
  MASS (MILLIGRAMS)
  MG/DNCM/STAGF
  CUM, PERCENT OF MASS SMALLER THAN 050
  CUM. (MG/ACM) SMALLER THAN D50
  CUM, (MG/DNCM) SMALLER THAN 050
  CUM, (GR/ACF) SMALLER THAN 050
  CUM, (GR/ONcF) SMALLER THAN DSC
  GEO, MfAN OIA, (MICROMETERS)
  DM/DLOGD (MG/DNCM)
  ON/OLOGD (NO. PARTICLES/DNCMJ
                                                            TABLE  22.
                                                         SAMPLING DURATION a  60,00 MIN
IMPACTOR TEMPERATURE •  eso.o F  n 343,3 c
STACK TEMPERATURE •  650,0 F « 343.3 C
 STACK PRESSURE = 28,20 IN, OF HG     MAX, PARTICLE DIAMETER = 100.0 MICROMETERS
6,40          CO •  0.00
        2.6651E-02 GR/DNCF

         SO        SI        82

         1         Z         3
       4,13      2,06      1,06
       0,41      0,34      0,09
                                 N2 • 71,36          02
                                     2.S624E+01  MG/ACM

                                     S3        S4        85
5,50           H20 • 15,00
        6,0987E*01 MG/DNCM

        56     FILTER
        7         8
      0.11
      0.25      1,05
                                   0.66      0,43      0,26
                                   0.16      0,35      0,26
     8,53E*00  7.06E*00  l,f*"*00  3,75E»00  7,29E*00  5,«1E*00  5.20E+00   2,19E*OJ

     l.OOE+02  8,60E»01  7,02  9.55E»03
     2,03E*01  2.93E+00  1.50E+00  9.61E-01  6.10E-01  3.47E-01  1.72E-01   7.51E-02
     6.17E«00  2.36E+01  6.53E«00  J.8(1E*01  Z.USEfOl  ?,B3Ei01  1.2UE+01   7,26Et01
     3.92E+05  5,04E*OB  1.04E+09  2.3lE»10  S.76E+10  S.60E+11  1,30E*»2   9.16E+IS
NORMAL (ENGINEERING 9T»NO»RO)  CONDITIONS ARE 21  DEC C AND 760MM HG,

-------
                                                               TABLE 23.
          0.1B  OT«09.76  0720  1PORT
      1MPACTOR FLOWRATE « 0,073 ACFM               IMPACTOR TEMPERATURE •  650.0 f • 313,3 C              SAMPLING DURATION *  60,00 MIN
      IMPACTOR PRESSURE DROP • 3.8 IN, OF HC       STACK TEMPERATURE *  650.0 f • 3U3.3 C
      ASSUMED PARTICLE DENSITY • 1,00 GM/CU.CM,     STACK PRESSURE * 28,20 IN, OF HG     MAX, PARTICLE DIAMETER « 189,2 MICROMETERS
      QA8 COMPOSITION (PERCENT)           C02 •  6,40          CO •  0,00           N| « 71,36          02 •  5,50           H20 « 15,00
      CALC, MASS LOADING • t.OSSSE-02 GR/ACF             2,665iE«02 OR/ONCF             2,368«E*01 MG/ACM             6,09B7E»01
      IMPACTOR ITAGE                                      so        si        82        sj        s«        ss        86     FILTER
      STAGE INDEX NUMBER                                  i         2         s         s         5         6         7         8
      D50  (MICROMETERS)                                 7,97      «,09      2,18      1,78      0,97      0,67      0,31
      MASS (MILLIGRAMS)                                 0,U1      0,34      0,09      0,18      0,35      0,26      0,25      1.05
      MG/DNCM/STAGE                                     8.s3E*oo  T.OSE+OO  i,87E+oo  3,7se«oo  7,?9E+oo  S,UIE*OO  S,?OE+OO
00
      CUM, PERCENT OF MASS SMALLER THAN DSO             i,ooE*o2  8,60E»oi  7,a«E*oi  T.IIE+OI  6,s2E»oi  s,32E+oi  «,a«E+oi
      CUM, (MG/ACM) SMALLER THAN DSO                    2,03E*01  1.76E+01  1,69E*01  l.SQEtOl  1.26E+01  1,05E*01  8,«7E+00
      CUM, (MG/DNCM) SMALLER THAN DSO                   5,2!E*01  «.5flE+Ol  «,35E*01  3,98E*01  3,25E«01  2,71E*01  ?,19E»01
      CUM, {GR/ACFJ SMALLER 7MAN DSO                    «,«8E»OS  T,68E»03  7,S6E«03  6.73E.03  5.SOE-03  U.5BE-03  3.70E-03
      CUM, (GR/ONCF) SMALLER TMAN 050                   2.29E-02  t,98E«02  1,90E«02  t,7«E-02  l,«2E«02  1.I8E-02  9.55E-03
      ceo. MEAN DIA, (MICROMETERS)                      S.SSE+OI  s,7te*oo  2,99E+oo  i,97E*oo  i,3iE»oo  s.oaE-oi  a,52E-oi  2,i6E»ot
      OM/DLOGD  (MG/D^CM)                                6.21E+00  2,U«E*01  6,87E«00  U.J6E+01  2.76E*01  i,S7E*01  1,53E«01  7,26E*OI
      DN/DLOGD  (NO, PARTICLE8/DNCM)                     2.0ZE+05  2,50E*08  «,9tE+08  1.0aE*10  2,3«E+10  1,2«E*11  3.17E+11  1.38E*13


     NORMAL (ENGINEERING STANDARD) CONDITIONS ARE 21 DEC C AND 760MH HG,

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                                                               TABLE  24.
           0.2B  OT.09.T6  1500  SPORT
       IMPACTOR  FLOWRATE • 0,073 ACFM               IMPACTOR TEMPERATURE »  620,0 F  • 326,7  c               SAMPLING DURATION  •  bo.oo  MJN
       IMPACTOR  PRESSURE PROP • s,» IN,  or HG       STACK TEMPERATURE •   620.0 r  • 326,7 c
       ASSUMED PARTICLE DENSITY • 3,58 GM/CU.CM.      STACK PRESSURE s 28,25 IN,  OF H6     MAX,  PARTICLE  DIAMETER  <*  100.0  MICROMETERS
       GAS  COMPOSITION (PERCENT)           C02 •   6.«0          CO •  0,00           N2  « 71,36          02  •   5,90           H20  «  19.00
       CALC,  MASS LOADING « J.8405E.OJ GR/ACF             9.6295E-OJ SR/ONCF             8.788SE+00  MG/ACM              2,2036E*01  MG/DNCM
       IMPACTOR  STAGE                                       so        n         s>2        33         su         ss        S6     FILTER
       STAGE  INDEX NUMBER                                  12305678
       050  (MICROMETERS)                                 A.09      2.06       1,07      0,85       0.43       0,28      0,11
       MASS (MILLIGRAMS)                                 0,01      0.11       0,11      0,11       0.23       0,23      0,13      0.16
to     MG/DNCM/8TAGE                                      2.02E-01   2.22E+00  2.22E+00  2.22EtOO  a,65E«00  4,65E*00  2.63E+00  1,23E*00
       CUM, PERCENT OF MASS SMALLER THAN oso              i,ooE+02   9,9iE»oi  8,'oE+oi.  7,89E+oi  6,88E+ot  «,77E»oi  2,66E»ot
       CUM, (MG/ACM) SMALLER THAN 050                    8.71C+00   7,82E*00  6.9JE+00  6,05E«00  03  3,03E»03  2,6aE>03  I.6JE-03  1.02E-03  5,6«E-oa
       CUM, (GR/ONCF)  SMALLER THAN OSO                   9.5UE-03   8.57E-03  7.60E-OJ  6.63E-03  U.59E-03  2,56E-03  1.U1E-OJ
       GEO, MEAN DIA.  (MICROMETERS)                      2.02E + Ol   2.91E + 00  1,01  6,OBE»01  3,(I8E>01  1.72E-01  7,52E>02
       OM/DLOGD  (MG/ONCM)                                1,«6E»01   7,a8E+00  7.78E+00  2,29E*01  1,57E*01  2,«5F*01  6.27E+00  1.07E+01
       ON/DLOGO  (NO, PARTICLES/ONCM)                      9,39E*03   1,63E»OB  1,27E*09  t,«OE*10  5.73E+10  3,11E*H  fc,52E*ll  I.35E+13


     NORMAL (ENGINEERING STANDARD) CONDITIONS ARE  21  DEC  C AND  760MM HG,

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     0-?B 07.09.7b  1500  SPORT
 IMPACTOR PLOWRATE * 0,071 ACFM
 IMPACTOR PRESSURE DROP * 3,9 IN, OF HG
 ASSUMED PARTICLE DENSITY »  1,00 6M/CU.CM.
 GAS COMPOSITION  (PERCENT)           C02 •  6.40
 CALC, MASS LOADING • S.840SE-03 GR/ACF
 IMPACTOR STAGE
 STAGE INDEX  NUMBER
 DSO  ("MICROMETERS)
 MASS  (MILLIGRAMS)
 MG/DNCM/STA6E
 CUM,  PERCENT OF  MASS SMALLER THAN  DSO
 CUM.  (HG/ACM)  SMALLER  THAN  050
 CUM,  (MG/ONCM) SMALLER THAN DSO
 CUM,  (GR/ACF)  SMALLER  THAN  DSO
 CUM,  (GR/DNcF) SMALLER THAN DSO
 GEO,  MEAN  DIA,  (MICROMETERS)
 DM/DLOGD  (MG/DNCM)
 DN/DLOGD  (NO,  PARTICLES/ONCM)
                                                  SAMPLING DURATION •  60,00 HI*
                TABLE  25.
IMPACTOR TEMPERATURE a  620,0 F s 326,7 C
STACK TEMPERATURF c  620,0 F s 336,7 C
 STACK PRESSURE « 28.25 IN, OF HG     MAX. PARTICLE DIAMETER • 169,2 MICROMETERS
       CO •  0,00
 9.6295E-03 OR/DNCF
  SO        31        82
  1         2         3
7,90      fl.OS      2,17
0,01      0,11      0,11
                                                           5,50
         H20 » 15.00
  2.2036E+01 MG/DNCH
  36     FILTER
  7         8
0,30
0.13      0,16
                            N2 • 71,36          02
                                8.78S3E+00 MG/ACM
                                S3        84        85
                                4         S         6
                              1,76      0,96      0,67
                              0,11      0,23      0,23
2.02E-01  2.22E+00  2,22E*00  2,22EfOO  «,65E+00  «,fc5E*00  2.63E400  3,23E*00
l.OOE+02  9,91E*01  8,90EtOi  7.89E+01  6,86EtOI  «,77E*01  2,66E*Ot
8,71E*00  7.82E+00  6,9SE*00  6.05E*00  O.J9E+00  2,34E»00  1,29E«00
2.18E+01  1.96E+01  l,74Et01  1.52E+01  i.OSEtOl  5,86E*00  JS.2UE+00
S.eiE-03  3,42E«03  3.03E-03  2.64E-03  1.63E-03  1.02E-03  5,64E»04
9,S4E*03  8.57E-03  7,60E>03  6.63E-03  4,59E>03  i,56E>03  1,41E'03
J.87E+01  5.66E+00  2.96E+00  1.95E+00  1.30E+00  8.00E.01  01  2.15E.01
1.47E-01  7.68E+00  8.17E+00  2.«7E*01  1,77P*01  2,91E*01  7.78E+00  1.07E*01
4,8SEt03  8,10E»07  S,99E*08  6,S3Et09  1.53E+10  1,09E*11  1,62E«11  2.05E+1?
NORMAL (ENGINEERING STANDARD)  CONDITIONS ARE  21  DEC  C  AND  760MM  HG,

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      0.3B 07.10-76  0635  SPORT
  IHPACTOR FLOWHATE • 0.066 ACFM
  IMPACTOR PRESSURE DROP •  J.2 IN,  OP HG
  ASSUMED PARTICLE DENSITY  • 1,58 6M/CU.CM,
  CAS COMPOSITION (PERCENT)           COS *   6.40
  CAUC, MASS LOADING • J.66S2E.01 GR/ACF
  IMPACTOR STAGE
  STAGE INDEX NUMBER
  D50 (MICROMETERS)
  MASS (MILLIGRAMS)
  MG/DNCM/STAGE
  CUM, PERCENT OF MASS SMALLER THAN D50
  CUM, (MG/ACM) SMALLER THAN D50
  CUM, (MG/DNCM) SMALLER THAN D50
  CUM, (GR/ACF) SMALLER THAN 050
  CUM, (GR/DNCF) SMALLER THAN 050
  GEO, MEAN DIA. (MICROMETERS)
  DM/DLOGD (MG/DNCM)
  DN/DLOGO (NO. PARTICLES/DNCMJ
                                                             TABLE  26.
                      SAMPLING DURATION c  60,00
IMPACTOR TEMPERATURE c  615,0 f • 323.9 C
STACK TEMPERATURE •  615.0 F t 323,9 C
 STACK PRESSURE • 28,28 IN, OF HG     MAX.  PARTICLE DIAMETER •  100.0  MICROMETERS
N2 s 71,36          02 *  5,50
    8,3826E*00 MG/ACM
    S3        SO        35
    «         5         6
                                                                          H20  «  15,00
                                                                   2,0699E*01  MG/DNCM
                                                                   56     FILTER
                                                                   7         8
       CO •  0.00
 9.1329E-OJ GR/DNCF
  SO        81        S2
  1         2         3
0,31      2,16      1,13      0,91      0,46      0,30       0,12
0.06      0,10      0.06      0,06      0.07      0,10       0.11      0,36
1.13E+00  I.22E+00  l.S3E»00  1,33E»00  1.56E*00  2,22E»00  2,45E*00   8,«5E»00
1,OOE*02  9,36E»01  8.30E+01  7,fe6E+01  7.02E*01  6.28E+01  5.21E+01
7,851*00  6,96E*00  6,«2E+00  5,8«E*00  5,26EtOO  4,37E*00  3,39E*00
1,96E*01  1,T3E*01  1.60E+01  l,47Et01  1.31E+01  1.09E+01  6.45E+00
3,«JE«OJ  3.DUE.OS  2.81E.03  2.57E-03  2.30E-03  1,91E>03  1.18E-OJ
8.55E-OS  7.58E-03  7.00E-03  6,«1E-03  5.73E-03  tt,76E>03  3.69E-03
2,08E*01  3.06E+00  1,57E*00  1,01E*00  6,«6E>01  3,74E*01  1.92E-01   6.64E-02
•9.77E-01  7,50E*00  4.69E+00  l,39E»Oi  5,3«E»00  1,20E«01  6,20EtOO   2.81E+01
5.63E+OU  1.39E+08  6.48E»08  7.13E+09  1.05E+10  1,22E»11  a,66E+ll   2,33Et)3
NORMAL (ENGINEERING STANDARD) CONDITIONS ARE SI  DEC C AND 760MM HG.

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                                                            TABLE  27.
     0-SB OT.10.7t  0635  SPORT
 IMPACTOR FLOWRATE »  0,86* ACFM                IMPACTOR  TEMPERATURE «   6i5,o  r  *  123,9  c               SAMPLING  DURATION  «   60,oo  *i*
 IMPACTOR PRESSURE DROP * 1.2  IN.  or  HG        STACK  TEMPERATURE  a  6is.o  F » 323,9  c
 ASSUMED PARTICLE DENSITY •  1,00 GM/CU.CM,      STACK PRESSURE  •  28.26  IN, OF HG     MAX, PARTICLE DIAMETER  •  189,2  MICROMETERS
 GAS COMPOSITION  (PERCENT)            C02  •   6.UO           CO •   0,00           NJ • 71,36          01  •   5,SO           H20  *  15,00
 CALC,  MASS  LOADING • 3.6632E.03 GR/ACF              9.1329E-03 GR/ONCF              8,S828E*00 MG/ACM              2.089»E»01  MG/DNCM
 IMPACTOR STAGE                                       so       si         82         33        so        ss        s&    FILTER
 STAGE  INDEX NUMBER                                   1         2         3          «         5         6          7         8
 050  (MICROMETERS)                                 «.30     «,27       2.28       1,86       1,02       0,71      0.3U
 MASS  (MILLIGRAMS)                                 0,06     0,10       0,06       0,06       0,07       0,10     0,11       0,38
 MG/ONCM/STAGE                                     1,33E*00  2,22E*00   1,33E+00   1,33E*00   1,56E*00   2,22E*00  2,«5E+00   8.BSE+00
 CUM,  PERCENT OF  MASS SMALLER  THAN 050             i,ooE+02  «,36E*oi   e,JOE*oi   7,66E+oi   7,o2e*oi   6,28E*oi  5,2ietoi
 CUM,  (MG/ACM)  SMALLER THAN  050                    7.85E+00  6,<)6E*00   6.12E+00   5.89E+00   5.26E+00   «,37E«00  3,39E^OO
 CUM,  (MG/DNCM)  SMALLER  THAN D50                   1.96E+01  1.73E+01   1.60E401   1.07E+01   1.31E+01   l,09Et01  8.U5E+00
 CUM,  (GR/ACF)  SMALLER THAN  D50                    3,«SE«03  3.0aE«03   2,81E«OJ   2.57E-03   2.30E-03   l,91E»03  1,USE-OS
 CUM,  (CR/DNCF)  SMALLER  THAN D50                   8.55E.03  7,58E-03   7.00E.03   6.41E-03   5.73E-03   4,76E>03  3.69E-03
 GEO,  MEAN  DIA,  (MICROMETERS)                      3,m*01  5,95E»00   3,12E + 00   2,06E + 00   1,38E + 00   8,51E«01  «,91E«01   2.01E-01
 DM/OLOGO (MG/DNCM)                                9,S2E»01  7,69E*00   <(,92E*00   1,«9E»01   5,96E*00   1,«2E*01  7,65E*00   2,81E*01
 DN/DL06D (NO,  PARTICLES/DNCM)                    3,01E+0«  6.97E+07   3,09E*08   3.25E+09   
-------
                          REFERENCES
1.   Tayler, Paul L.,  Characterization of Copper Smelter Flue
    Dust, APCA Paper 76-24.3, presented at the 1976 Annual
    Meeting of the Air Pollution Control Association.

2.   Smith, Wallace B., et al, Particulate Sizing Techniques for
    Control Device Evaluation, Appendix A., U.S. Environmental
    Protection Agency Report EPA-650/2-74-102a prepared by
    Southern Research Institute under Contract No. 68-02-0273.
                              63

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                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing)
I. REPORT NO.
   EPA-600/2-80-151
                              2.
                                                            3. RECIPIENT'S ACCESSION NO.
4. TITLE AND SUBTITLE
Evaluation of an Electrostatic Precipitator for Control  of
Emissions from a Copper  Smelter Reverberatory Furnace
                                                            \S. REPORT DATE
                                                             __  JUNE 1980 ISSUING DATE,
                                                            |6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S)
G. B.  Nichols, j.
                                                            8. PERFORMING ORGANIZATION REPORT NO.
                     McCain,  J.  E. McCormack, W. B.  Smith
9. PERFORMING ORGANIZATION NAME AND ADDRESS
I
Southern Research Institute
2000 Ninth Avenue, South
Birmingham, Alabama    35205
                                                            10. PROGRAM ELEMENT NO.
                                                               1AB610
                                                            11. CONTRACT/GRANT NO.
                                                                 R804762
12. SPONSORING AGENCY NAME AND ADDRESS
Industrial Environmental  Research Laboratory
Office of Research and  Development
U.  S.  Environmental Protection Agency
Cincinnati, Ohio   45268
                                                            13. TYPE OF REPORT AND PERIOD COVERED
                                                            14. SPONSORING AGENCY CODE
                                                               EPA/600/12
15. SUPPLEMENTARY NOTES
Project Officer:  John  0.  Burckle
 16. ABSTRACT
      This report describes tests to evaluate  the  performance of an electrostatic
precipitator installed  on a copper reverberatory  furnace.   Particle size measurements
were  made with modified Brink cascade impactors in order to calculate the ESP fractional]
efficiency.  The particle size distributions  at the inlet  and outlet were both found
to  be bimodal.  The overall mass median diameter  of the inlet distribution was greater
than  10  ym.  The SRI-EPA computer model was  used to simulate the ESP performance.
Values of the mass collection efficiency were found by instack filters to be 96.7%, and
by  cascade impactors  to be 96.6%.  The computer model predicted an overall efficiency
to  be 96.8%, which is also the design efficiency.   The particulate matter was found
to  be very cohesive and hygroscopic, and the  composition (color) varied from impactor
stage to stage.  There  was no evidence of electrical problems due to particle
resistivity or space  charge.  Simultaneous testing was also carried out by Radian
Corporation, Austin,  Texas.  Results of the Radian study are included in a report
"Trace Element Study  at a Primary Copper Smelter,  Vol. I and II" (EPA-600/2-70-065a
and - 065b, March 1978).
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                               b. IDENTIFIERS/OPEN ENDED TERMS
                                                                         c.  COSATI Field/Group
Exhaust  Emissions
Smelting
Trace  Elements
Pollution
                                               Copper  Smelter
                                               leverberatory Furnace
                                               Particulate  Emission
                                               Slectrostatic Precipitator
                                               Field Test
                                               fractional Efficiency
      13B
18. DISTRIBUTION STATEMENT
Release  to  Public
                                               19. SECURITY CLASS (This Report)'
                                                 Unclassified
21. NO. OF PAGES
       72
                                               20. SECURITY CLASS (Thispage)
                                                 Unclassified
                                                                         22. PRICE
EPA Form 2220-1 (Rev. 4-77}
                       PREVIOUS EDITION IS OBSOLETE

                                            64
                                                          * U.S. GOVERNMENT PRINTING OFFICE:  1980—857-165/0016

-------