oEPA
         United States
         Environmental Protection
         Agency
          Industrial Environmental Research  EPA-600/7-78-177b
          Laboratory          December 1978
          Research Triangle Park NC 27711
University of Washington
Electrostatic Scrubber
Tests at a  Coal-fired
Power Plant

Interagency
Energy/Environment
R&D Program Report

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                  RESEARCH REPORTING SERIES


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 This report has been assigned to  the INTERAGENCY ENERGY-ENVIRONMENT
 RESEARCH AND DEVELOPMENT series. Reports in this series result from the
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                                EPA-600/7-78-177b

                                    December 1978
  University of Washington
Electrostatic  Scrubber Tests
 at a  Coal-fired  Power  Plant
                      by

               M.J. Pilat and G.A. Raemhild

                University of Washington
              Department of Civil Engineering
               Seattle, Washington 98195
                 Grant No. R804393
              Program Element No. EHE624A
             EPA Project Officer: Dale L. Harmon

           Industrial Environmental Research Laboratory
            Office of Energy, Minerals, and Industry
             Research Triangle Park, NC 27711
                   Prepared for

          U.S. ENVIRONMENTAL PROTECTION AGENCY
             Office of Research and Development
                Washington, DC 20460

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                             Abstract
A 1000 acfin University of Washington Electrostatic Spray Scrubber pilot
plant was tested on the coal fired boiler unit no. 2 at Centralia Power
Plant to demonstrate its effectiveness for controlling the emissions of
fine particles.  The multiple pass, portable, pilot plant operates by
combining oppositely charged aerosol particles and water droplets in
two spray towers.  Aerosol charging sections at a negative polarity pre-
cede each spray tower.  The pilot plant was operated at gas flows beyond
its rated capacity.  Inlet gas flow as high as 1600 acfm were recorded.
Tests to determine the effect of reducing the size of the unit were
performed.  The scrubber was operated and tested in two operating modes.
The two stage mode included two active particle charging corona sections
and two spray towers.  The one stage mode utilized only one corona
section:and one spray tower.

Simultaneous inlet and outlet source tests utilizing University of
Washington Cascade Impactors and in-stack filters provided both size-
dependent and overall mass basis particle collection efficiency informa-
tion.  Measured overall particle collection efficiencies ranged from
99.30 to 99.99% depending upon scrubber operating conditions and the
inlet particle size distribution and mass concentration.  Particle mass
concentrations measured at the scrubber outlet ranged from ,00018 grains/
sdcf to .00116 grains/sdcf.  The average overall  particle collection
efficiency for all tests performed in the two stage mode was 99.93%
while the one stage average efficiency was 99.825%.  An integrating
nephelometer was utilized at the scrubber outlet because of low outlet
mass concentrations and subsequent low sample weights.  The light
scattering coefficient was measured as a relative indication of outlet
mass concentration for different operating parameters.  Tabular and
graphical  data is presented to illustrate the size dependent and overall
collection efficiencies for all  tests performed.

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                               Contents
                                                                     Page
Abstract                                                              til
Contents                                                               iv
List  of Figures                                                        vi
List  of Tables                                                       viii
Acknowledgements                                                       ix
Abbreviations and Symbols Used                                          x
I.     SUMMARY AND CONCLUSIONS                                          1
II.    RECOMMENDATIONS                                                  2
III.   RESEARCH OBJECTIVES                                              3
IV.    DESCRIPTION OF SOURCE                                            4
V.     DESCRIPTION OF UW ELECTROSTATIC SCRUBBER APPARATUS               7
       A.  Review of Previous Work                                      7
       B.  Description of Overall System                                7
       C.  Cooling Tower                                                9
       D.  Particle Charging Corona Section                             9
       E.  Water Spray Towers                                          12
       F.  Mist Eliminator                                             14
       G.  Tests Ducts                                                 14
       H.  Fan                                                         14
       I.  High Voltage Power Supplies                                 16
       J.  Water Supply System                                         16
       K.  Purge Air Heating System                                    17
VI.    EXPERIMENTAL PROCEDURES AND TEST EQUIPMENT                      20
VII.   PARTICULATE COLLECTION EFFICIENCY RESULTS                       23
       A.   General Test Description                                    23
       B.   Particulate Collection Efficiency (Two Stage Mode)           23
           1.   Cascade Impactor Measurements                           23
           2.   In-stack Filter Measurements                            26
                                  TV

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                           Contents (cont.)

                                                                  Page
       C.  Participate Collection Efficiency (One Stage Mode)      32
           1,  General System Description                          32
           2.  In-Stack Filter Measurements                        32
           3.  Cascade Impactor Measurements                       38
           4.  Integrating Nephelometer Measurements               41
VIII. REFERENCES                                                   43
APPENDIX A                                                         44
       Detatls on Sampling Techniques                              45
APPENDIX B                                                         46
       Converting Units of Measure                                 47

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                           List of Figures

                                                                    Page

 IV-1    Photograph of UW Electrostatic Spray Scrubber Located
        at Boiler Unit No. 2, Centralia Power Plant                   5

 IV-2    Schematic of Ducting Arrangement to UW Electrostatic
        Spray Scrubber Pilot Plant at Centralia Power Station         6

 V-l     General Layout of Electrostatic Scrubber Pilot Plant          8

 V-2     Cooling Tower Schematic                                      10

 V-3     Particle Charging Corona Section                             11

 V-4     Collection Plate Flushing System                             13

 V-5     Spray Header and Nozzle Arrangement Typical to Spray
        Towers #1 and #2                                             15

 V-6     Charged Liquor Recycle System                                18

 V-7     Heated Purge Air System                                      19

 VI-1    UW Cascade Impactor Sampling Train                           22

 VII-1   Particle Collection Efficiency and Penetration vs.
        Particle Size for Impactor Tests 3-8 (Two Stage System)      25

 VII-2   Particle Mass Concentration for Particles Less Than
        Stated Diameter for Impactor Tests 3-5                       26

 VII-3   Particle Mass Concentration for Particles Less Than
        Stated Diameter for Impactor Tests 6-8                       27

 VII-4   Inlet and Outlet Particle Size Distributions for
        Cascade Impactor Tests 3-5 (Log-Normal Approximation)        29

 VII-5   Inlet and Outlet Particle Size Distributions for
        Cascade Impactor Tests 6-8 (Log^Normal Approximation)        30

 VII-6   Particle Collection Efficiency and Penetration vs.
        Particle Size for Impactor Tests 12-18 (One Stage System)    35

VII-7   Particle Mass Concentration for Particles Less Than
        Stated Diameter for Impactor Tests 12-15                     36

VII-8   Particle Mass Concentration for Particles Less Than
        Stated Diameter for Impactor Tests 16-18                     37

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VII-9   Inlet and Outlet Particle Size Distributions for
        Cascade Impactor Tests 12-15 (Log-Normal Approximation)      39

VII-10  Inlet and Outlet Particle Size Distributions for
        Cascade Impactor Tests 16-18 (Log-Normal Approximation)      40

VII-11  Light Scattering Coefficient,  Bscat,  Measured at the
        Outlet of the UW Electrostatic Spray Scrubber for Various    42
        Spray Voltages (All Other Parameters Held Constant)
                                 VTT

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                            List of Tables


                                                                   Page

V-l     High Voltage Power Supply Units.                            16

VI-1    Participate Source Test Parameters and Measurement
        Techniques.                                                 20

VII-1   Results of Cascade Impactor Tests 3 Through 8 at
        Centralia Power Plant (Two Stage System).                    24

VII-2   Results of Simultaneous In-stack Filter Tests 1-F
        Through 8-F at Centralia Power Plant (Two  Stage
        System).                                                     31

VII-3   Results of Simultaneous In-stack Filter Tests 9-F
        Through 16-F at Centralia Power Plant (One Stage
        System).                                                     33

VII-4   Results of Simultaneous Impactor Tests 12-18,
        Centralia Power Plant (One Pass System).                     34

VII-5   Comparison of Incremental  Particle Collection
        Efficiencies Between the Two Stage and One Stage
        System.                                                     41
                                vn

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                         ACKNOWLEDGEMENTS
The authors wtsh to express their appreciation for the assistance
and cooperation of the Project Officer, Mr.  Dale Harmon,  Chemical
Engineer in the Particle Technology Branch of the Environmental
Protection Agency.  The cooperation of Bob Werner, Gary Slanina,
Ted Phillips, and Tom White of Pacific Power and Light Co.  is also
greatly appreciated.

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              ABBREVIATIONS AND SYMBOLS USED

SCA                          Specific collection area (ft2/scfm)
L/G                          Liquid to gas ratio (gallons/1000 scfm)
dj-Q                          Aerodynamic cut diameter of cascade
                             impactor stages (microns)
y                            Gas viscosity (gm/cm-sec)
D.                           Jet diameter (cm)
 J
I|VQ         .                 Inertial impaction parameter at 50% col-
                             lection efficiency for particles of dia-
                             meter d5Q
C                            Cunningham correction factor
V.                           Gas velocity in the jet (m/sec)
                                                            -1
B   .                         Light scattering coefficient (m  )

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                            Section 1

                     SUMMARY AND CONCLUSIONS
The University of Washington Electrostatic Spray Scrubber portable pilot
plant was tested at the Pacific Power and Light Power Plant in Centralia,
WA on coal fired boiler unit no. 2 to demonstrate its effectiveness in
controlling the fine particle emissions.  The pilot plant consists of a
cool.ing tower, two corona sections which charge the particles to a nega-
tive polarity, two spray towers into which positively charged water
droplets are sprayed and on electrostatic mist eliminator.

The unit was operated and tested in two operational modes.  The two
stage mode utilized both particle charging corona sections and both
charged droplet spray towers while the one stage mode utilized only
one corona section and one spray tower.  Overall particle collection
efficiencies measured for the two stage mode ranged from 99.30% to
99.99% at corona section specific collection areas (SCA) of 0.050 to
0.068 ft2/scfm.  Overall particle collection efficiencies for one stage
operation ranged from 99.50% to 99.89% at an SCA range of .024 to .037
ft2/scfm.  The UW Electrostatic Scrubber SCA range from about 0.024 to
0.068 ftVscfm is significantly less in magnitude than the corresponding
efficiency electrostatic precipitator with an SCA range of 0.3 to 0.8
ft2/scfm.

In conclusion it is apparent that the UW Electrostatic Spray Scrubber is
effective in the collection of particulate emissions from a coal fired
boiler.  A 37% reduction in active length of the scrubber resulted in
particle collection efficiencies still in excess of 99%.  The effect of
this size reduction, from a full scale design point of view, results in
a decrease in both capital  and operating costs of the unit while main-
taining high overall particle collection efficiencies.

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                            Section II

                         RECOMMENDATIONS
To better evaluate the UW Electrostatic Spray Scrubber performance on a
coal fired boiler, it is recommended that additional fan capacity be added
to the system to provide a greater volumetric gas flow rate.  This would
result in an even shorter gas residence time and greater particle mass
concentrations at the scrubber outlet sampling port.  An increased mass
concentration at the outlet would result in greater sample weights and
consequently greater statistical reliability in the data.  The process
changes and system perturbations apparent in the Centralia tests would
also have less of a relative effect upon the results.

We also recommend that the pilot plant be used to demonstrate its effec-
tiveness for simultaneous control of particulate and S02 emissions from
coal fired boilers.  To accomplish this, it is felt that the installation
of continuous S02 monitoring equipment would expedite the study as well
as increase the accuracy of the measurements.

Design and construction of a larger, improved liquor recycle system is
also recommended.  This would be particularly appropriate for an S02
study.

Future considerations should be given to design and installations of a
larger scale (10,000 acfm) pilot plant or demonstration unit with a self
contained liquor recycle system.

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                            Section III

                        RESEARCH OBJECTIVES
The primary objective of the field tests at Pacific Power and Light's
Centralia Power Plant was to determine the effectiveness of the UW
Electrostatic Spray Scrubber in controlling fine particle emissions from
a coal fired power boiler.  Simultaneous inlet/outlet particulate collec-
tion measurements provided the basis for this study.

The effect of a variation in certain scrubber operating parameters (gas
residence time, SCA, L/G, and applied voltages) on particle collection
efficiency was also an objective of this research.  This information would
then be used in the design and economic analysis of a full  scale retrofit
system for a coal fired boiler.

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                              Section IV

                      DESCRIPTION OF THE SOURCE
The Centralia Steam-Electric Project located near Centralia, Washington is
a coal fired electric power generating station owned by eight Northwest
utilities and operated by Pacific Power and Light Company personnel.  The
plant contains two units which have a combined generating capacity of
1,330,000 kilowatts of electricity (665,000 kilowatts per unit).  The two
boilers, manufactured by Combustion Engineering, are pulverized coal fired
type, each with a designed steam rate of 5,200,000 pounds per hour at
2400 psig at the turbine inlet.  The two turbine generators were manufactured
by Westinghouse Electric Corporation, each with a guaranteed rating of
664,898 kilowatts.  The primary fuel  is sub-bituminous C coal which comes
from a strip mine adjacent to the plant.  The coal is low in sulfur content
(0.5 - 0.75%) and has a design heating value of 8100 BTU's per pound.  Fly ash
particulate emission is controlled by two electrostatic precipitators.

In October, 1977, the U of W Electrostatic Spray Scrubber was transported
to the Centralia Power Plant.  The sample gas stream (approximately 1500 acfm)
was tapped from the outlet of boiler unit number 2.   A 12 inch sampling
scoop was installed (facing upstream) at the center point of the transition
duct between the air preheater and the precipitator.   Ten inch diameter
aluminum ducting connects the sampling scoop to the scrubber which is located
approximately 60 feet below on the ground level.  Due to the high negative
static pressure in the main duct, a Dayton centrifugal  blower was installed
at the scrubber inlet to boost the air flow capabilities.  Figure IV-1 shows
the location of the scrubber trailer (on the right)  and the laboratory
trailer (on the left).  A schematic of the ducting arrangement showing the
lengths of duct from the sampling scoop to the inlet of the pilot plant is
shown in Fig. IV-2.

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en
                          Fig. IV-1.  Photograph of UW Electrostatic Spray Scrubber Located
                                      at Boiler Unit No. 2, Centralia Power Plant

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        .Air  Preheater
                              Precipitator
            59'
                                                                   Sampling
                                                                   Port
                                       Scrubber
                         Ducting  Arrangement  to  UW Electrostatic  Spray Scrubber
                        MATERIAL:
                          10"  Dia.  Aluminum
                          Ducting
                        TOLERANCE:

                           .X ±
                          .XX ±
.XXX ±
            UNIVERSITY OF  WASHINGTON
              DEPARTMENT OF CIVIL ENGINEERING
           DRAWING NO.
           DRAWING BY:
           APPROVED BY:
SCALE:
DATE:
                                  6/27/78
DATE:
Fig. IV-2.  Schematic of Ducting Arrangement to UW Electrostatic Spray
            Scrubber Pilot Plant at Centralia Power Station
                                  6

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                              Section V

          DESCRIPTION OF UW ELECTROSTATIC SCRUBBER APPARATUS
A.  Review of Previous Work

    Penney (1944) patented an electrified liquid spray test precipitator
    involving particle charging, by corona discharge and droplet charging
    by either ion impaction or induction.  Penney1s system consisted of
    a spray scrubber with electrostatically charged water droplets col-
    lecting aerosol particles charged to the opposite polarity.  Kraemer
    and Johnstone (1955) reported theoretically calculated single droplet
    (50 micron diameter droplet charged negatively to 5,000 volts) col-
    lection efficiencies of 332,000% for 0.05 micron diameter particles
    (4 electron unit positive charges per particle).  Pilat, Jaasund, and
    Sparks (1974) reported on theoretical calculation results and labora-
    tory tests with an electrostatic spray scrubber apparatus.  Pilat
    (1975) reported on field testing during 1973-74 with a 1,000 acfm UW
    Electrostatic Scrubber (Mark IP model) funded by the Northwest Pulp
    and Paper Association.  Pilat and Meyer (1976) reported on the design
    and testing of a newer 1,000 acfm UW Electrostatic Scrubber (Mark 2P
    model) portable pilot plant.   Pilat, Raemhild, and Prem (1978) reported
    on tests of the UW Electrostatic Scrubber at a steel  plant.  The UW
    Electrostatic Scrubber (Patent Pending) has been licensed to the Pollu-
    tion Control  Systems Corporation (of Renton and Seattle, Washington)
    for production and sales.


3.  Description of Overall System

    The major components of the pilot plant include a gas cooling tower,
    an inlet and  outlet test duct, two particle charging corona sections,
    two charged water droplet spray towers, and a mist eliminator.  Aux-
    iliary equipment includes transition ductwork between major components
    and a fan.   The pilot plant is housed in a 40 ft.  long trailer and can
    be easily transported to different emission sources.

    The general  layout of the pilot plant is shown in Figure V-l.   Incoming
    gases enter the top of the trailer to be treated in the vertical  gas
    cooling tower and then turn vertically upward to enter the inlet test
    duct.   After  moving down through the inlet test duct, the gases enter
    the first of  three horizontal  passes.

    The first pass contains both  particle charging corona sections and the
    first of two  water spray towers.   The two coronas are at either end of
    this pass and are separated by spray tower #1.   Spray tower #2 comprises
    the entire second horizontal  pass and the last (third) pass contains the
    mist eliminator.

    At the outlet of the third horizontal pass, the gases enter the top of
    the outlet test duct and are  then directed to the fan before being
    exhausted through the trailer roof.

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    INCOMING
     GASES
CO
                         INLET TEST  DUCT
                              SPRAY  TOWER NO. 2
                                  CORONA NO. I
                                                         EXHAUST
                                                          CASES
                                                                    SECTION A-A

                                                              CROSS SECTIONAL VIEW OF
                                                           THREE WSS  HORIZONTAL SECTION
                                                                                                  OUTLET  TEST DUCT
                                                                  MIST
                                                               ELIMINATOR
SPRAY  TOWER NO, I
                                                              ELEVATION VIEW
                        .	SPWAY TOWER NO. 2
                                                                                                                      FAN
                             Fig. V-l.   General  Layout of  Electrostatic Scrubber  Pilot Plant

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C.  Cooling Tower

    The cooling tower is designed to lower the gas temperature to below
    250°F in order to maintain structural  integrity of the system
    which is constructed of steel and fiberglass reinforced plastic.   The
    cooling tower, as shown in Figure V-2  is 1 ft. 2 in.  in diameter x
    9 ft. 8 in. in height and is constructed of 21 gage T. 304 stainless
    steel.   Cooling water is introduced through four ports spaced at 2 ft.
    intervals on one side of the tower and is sprayed vertically upward
    from the tower's center!ine.  Four Bete Model  W 10080 F full cone
    stainless steel nozzles used for spraying are  capable of delivering
    up to 3.0 gpm at 50 psig.  A funnel built into the bottom of they
    spray tower extends through the trailer floor  for cooling water re-
    moval .
D..  Particle Charging Corona Sections

    Particle charging corona sections are located at either end of the
    first horizontal  gas passage.   The corona shells are constructed from
    3/16 in. wall  thickness fiberglass reinforced plastic (FRP) with in-
    terior dimensions of 2 ft.  wide x 3 ft.  6 in. high x 5 ft.  long in
    the direction  of gas flow.   Access to a  corona interior is  through
    removable 2/16 in.  FRP end  plates which  are normally bolted to 2 in.
    full perimeter face flanges on either end of a corona.

    The coronas are designed to operate in either a single or double lane
    gas passage mode.  Switching from one to another requires rearrangement
    of the adjustable collection plates and  discharge frame(s).  The width
    of individual  gas lane(s)  for either mode is maintained at  1  ft. and
    the discharge  frame to collection plate  spacing is therefore 6 in.  Fig-
    ure V-3 shows  a cutaway schematic of a corona set up for single lane
    operation.   The testing at  Centralia Power Plant was performed with
    single lane corona  section.                                     u

    The overall dimensions of the discharge  frame shown in Figure V-3 are
    27-1/2 in.  high x 3 ft. 9  in.  long.  The frame is constructed of 1/4 in.
    x 3/4 in.  T. 304 stainless  steel  rectangular bar stock members.   Prior
    to the Centralia test program these frames were modified by welding
    1/8 in.  diameter stainless  steel  rods in 1-3/4 in. lengths  perpendicular
    to the vertical members of  each discharge frame.   The spikes  have
    sharp points on both ends and are welded at 2 in. intervals.   This
    modification has decreased  the plate to  frame spacing by 1/4  in.

    The collection plates shown in Figure V-3 are 41-1/4 in.  high x 59 in.
    long and are constructed from 11  gage T.  316 stainless steel.   The
    plates serve as full  chamber baffles to  keep the gases within the con-
    fines of the single lane passage.

    A negative  corona is used to charge the  particles negatively.   This is
    accomplished by maintaining the discharge frame(s) at a high  negative

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                    REMOVABLE  GROUND PLATE (S.S.)
                      FOR ONE LANE  OPERATION
HIGH VOLTAGE
FEEDER  CABLE
              HIGH
        VOLTAGE  INSULATOR
          DISCHARGE FRAME
           SUSPENSION  ROD
     HIGH VOLTAGE
    DISCHARGE  FRAME
  GAS  INLET
AND  OUTLET OPENING
                                                                 PURGE AIR  DUCT
                                                                   FRP WALLS
                                                    S.S. GROUND PLATE (OUTER)
                                                    FOR TWO LANE OPERATION
                                                       Stainless Steel- Discharge Spikes
                          GROUND PLATE ALIGNMENT
                            AND SUPPORT BARS
                        Fig. V-3.  Particle Charging Corona Section

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    potential and the collection plates at a neutral or ground potential.
    Field strengths generated in corona #1 and corona #2 are 13.65 KV/in.
    and 15.61 KV/in. respectively.  Corona power supplies are discussed
    in a later section.  The discharge frame is electrically isolated
    from all other components inside the corona.  This isolation is pro-
    vided by suspending the frame on two 1 in. diameter T. 303 stainless
    steel rods which are connected to porcelain insulators.  The Cerama-
    seal Model 902B1353-6 insulators are housed in 1 ft. diameter x 2 ft.
    long x 1/4 in. wall thickness plexiglass tubes which are centered
    3 ft. 6 in. apart and are located on top of the corona shells.  Two
    1 ft. to 1 ft. 2 in. x 3 in. FRP reducing flanges are used to join
    the plexiglass tubes to the corona top.

    The insulators are continually flushed with a supply of heated purge
    air.  The temperature of the purge air is maintained at about 120°F
    and an even flow across a plexiglass tube section is obtained by
    introducing the purge air through a distribution plate having approxi-
    mately 10% hole area.  The flushing face velocity of the purge air
    is set at about 0.6 ft/sec.   This same purge air distribution flange
    discharge frame(s), is bolted directly to it.   The high voltage lead-
    in to the discharge frame is through one of the two feed-through type
    insulators.

    The collection plate and discharge frame flush system is shown sche-
    matically in Figure V-4.  A continuous wall wash is supplied to the
    collection plates through 1  in.   FRP square tube which had 1/8 in.
    diameter holes drilled diagonally into the corner adjacent the
    collection plate.  The discharge frame flush is an intermittent spray
    supplied by two Bete 80° fan nozzles.   Both corona section and the
    mist eliminator are equipped with this flushing system.

    At the nominal gas flow rate of 1,000 acfm, the gas velocity in the
    corona is 4.76 ft/sec for single lane operation and 2.38 ft/sec for
    double lane operation.  The corresponding gas  residence times are
    1.05 and 2.10 seconds.  By varying the volume  of air flow through
    the system, however, the gas residence time can range from 0.70 sec-
    onds (single lane operation at 1,500 acfm to 4.20 seconds (double
    lane operation at 500 acfm).


E.  Water Spray Towers

    The first of two spray towers used in  the pilot plant is situated in
    the middle of the first horizontal  gas passage (between the two coronas)
    while the second spray tower comprises the entire horizontal  gas  pas-
    sage.   Both spray towers are 3 ft.  in  diameter x 3/16 in wall thick-
    ness and are constructed from FRP.   The lengths of the two spray
    towers are 10 ft. and 24 ft. for tower #1 and  #2 respectively.   Gas
    velocity in the spray towers at  a nominal gas  flow of 1000 acfm is
    2.36 ft/sec.   Corresponding gas  residence times are 4.24 and 10.17
    seconds for towers #1 and #2 respectively.


                                 12

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Collection Plate Flush
                              COLLECTION PLATES
                              (SINGLE LANE OPERATION)
                                                                   PURSE AIR AND HIGH
                                                                   VOLTAGE ENTRY (PURGE
                                                                   AIR  DUCTS, INSULATORS,
                                                                   SUSPENSION RODS AND
                                                                   DISCHARGE FRAME) OMITTED
                                                                   FOR CLARITY
                                                                   Discharge Frame Sprays
CORONA SHELL
                     Fig,  V-4,  Collection Plate Flushing System

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    Utilizing a single spray header in each tower, a maximum of 21 nozzles
    can be used in the two towers.  The total number of nozzles used can
    vary depending on the type of nozzle, the total water flow rate and
    the pressure head desired.  All nozzles spray in the direction of gas
    flow (co-currently).  A maximum of 6 nozzles can be used in spray
    tower #1 although only the 3 nozzles located farthest upstream were
    used to avoid flooding of corona section #2 with spray droplets.  A
    single spray header in spray tower #2 can accommodate a maximum of
    16 nozzles.  A total of 5 to 12 nozzles were used in the Centralia
    tests depending on the desired flow rate.  Bete L-80 spiral fog nox-
    zle/header arrangement typical for both spray towers #1 and #2 is
    shown schematically in Figure V-5.

    A positive charge is imparted to the water droplets by maintaining
    the nozzles at a positive potential (direct charging).  The nozzles
    are electrically isolated from the spray tower walls by introducing
    heated purge air through 3 in. diameter x 4 in. long polyvinyl
    chloride (PVC) entry caps which are situated on top of the two
    spray towers (see Figure V-5).  Both the water and the high voltage
    lead-in cable enter through a 1/4 in. diameter street tee fitting
    connected to the middle of each entry cap.
F.  Mist Eliminator

    The mist eliminator is situated in the middle of the third and last
    horizontal pass and is used to remove entrained water droplets from
    the airstream.  The mist eliminator is identical to the corona sec-
    tions with the exception of the discharge frame being maintained at a
    positive potential and the total height being 2 in. shorter (neces-
    sitating an equivalent shortening of the discharge frame and collec-
    tion plates).
G.  Test Ducts

    The inlet and outlet test ducts are located immediately before the
    first corona and immediately after the mist elinimator respectively
    (see Figure V-l).  Both test ducts are constructed from 3/16 in. wall
    thickness FRP and are 12 in. in diameter x 4 ft.  long.  Vertical gas
    flow in a downward direction is employed because it allows the most
    convenient positioning of the particle sizing source test equipment
    used and described in Section VI, "Particulate Sampling Apparatus."
    The particle sizing source test equipment also dictated the size of
    the test ports which are 6 in.  wide x 1  ft. 6 in.  high.  The test
    ports are located three duct diameters downstream and one duct dia-
    meter upstream from flow disturbances.
H.   Fan

    The fan used to induce the air flow (i.e., clean side) through the
    pilot plant is a New York Blower Model  RFE-12.   The straight-bladed

                                  14

-------
                        WATER HIGH
                        VOLTAGE  AND
                     PURGE AIR ENTRY
                     CAP
Fig. V-5.  Spray Header and Nozzle Arrangement Typical
        to Spray Towers #1 and #2.

-------
     fanwheel  and  housing  are  constructed  from  FRP.  The  fan  is driven
     through  a split  pulley  belt  drive  by  a Westinghouse  5 H.P.,  208  volt,
     3-phase  motor .turning at  1,800  rpm and is  capable of delivering  up  to
     1,500  acf.m at 8  in. water column  (WC) static pressure.   The  fan  has a
     horizontal  inlet and  vertical outlet.  A 3/16  in. FRP wall thickness x
     1  ft.  diameter exhaust  duct  containing an  adjustable damper  extends
     up through the trailer  roof.

     As previously mentioned,  a Dayton  centrifugal  blower was installed
     at the scrubber  inlet to  increase  the air  flow capabilities  at the
     Centralia Power  Plant.
 I.  High Voltage Power Supplies

    Four high voltage power supply units used in the pilot plant serve the
    coronas, mist eliminator, and water droplet charging.  All four units
    operate off a 110 volt, 50 Hz, 1 0 supply and are equipped with multi-
    range voltage and current meters on the high voltage output side.  The
    units are also equipped with overvoltage and overcurrent surge protection.

    The power supplies used for the two corona sections are equipped with
    spark rate controllers.  The Universal Voltronics unit which energizes
    corona #1 has a L.L. Little P-30 automatic voltage control and the NWL
    unit for corona #2 has an integrated NWL spark rate controller.  The
    four power supplies are described in the following table.
                Table V-l.   High Voltage Power Supply Units.
Source
Corona #1
Corona #2
Mist Eliminator
Droplet Charging
Model
Universal Voltronics
NWL
Hipotronics #860-16
Hipotronics #825-40
Polarity
Negative
Negative
Positive
Positive
Rated Peak
Output
KV
40
90
60
25
mA
25
30
16
40
0.  Water Supply System

    The water supply system for the scrubber is controlled with a single
    control  panel situated,near the inlet sampling port.   Two different
    sources  supply water to the control panel:  charged.water (either
    recycled or fresh) and uncharged fresh water.   The charged water is
    used as  scrubbing liquor in spray towers #1 and #2 and the uncharged
    water is used for the corona flushing systems  and the cooling tower.

                                 16

-------
   A schematic of the charged scrubbing liquor system is shown in Figure
   V-6.  The arrangement illustrated in Figure V-6 is for recycled liquor
   with fresh water make up.  The Centralia Power Plant tests were per-
   formed with fresh (not recycled) water.   The 3 in. drain to the set-
   tling tank (#3) was disconnected and ducted to the power plant water
   treatment system.  Fresh water was then supplied to the settling tank
   at the same consumption rate as supplied to spray towers #1 and #2
   combined.

   A Goulds centrifugal  pump model 3196 ST provides the necessary liquor
   flow requirements of 95 psig and a total flow rate of 17 gpm.   A
   maximum flow of 5 gpm is provided to spray tower #1 while a maximum
   of 12 gpm is supplied to spray tower #2.

   The water in the settling tank (either  recycled or fresh) is trans-
   ferred into the sump tank by a 1 $ Deming centrifugal  pump through the
   recycle sump sprays.

   The fresh water supply is used in the gas cooling tower (approximately
   3 gpm) and the corona section flush systems (flow rate is unmonitored).


K.   Purge Air Heating System

   The new purge air heating system is schematically illustrated  in Figure
   V-7.  The system consists of both commercially available and custom
   built components.  The fan is a Barry Blower model BUF-90 Junior Fan
   employing a 1/3 HP motor with a maximum capacity of 500 cubic  feet per
   minute.   The discharge air then passes  through a custom design Nelco
   Duct Heater.   It is a 9 Kw heating unit with 4 stages to regulate the
   degree of heating required.   The duct heater operated on 208V, 3 power
   with a 110V control  source which is external  of the heater. A custom
   designed distribution plenum follows the heater and provides an adjus-
   table purge air supply to the high voltage access points on the two
   corona sections, the  mist eliminator section and the  recycle sump tank.
   The basic design criterion for the purge air system is to provide 150°F
   purge air at a range  of up to 500 acfm  (total).
                                17

-------
            LIQUOR  FLOW- RATE
            CONTROL BOARD
      FRESH
      WATER
      MAKE-
ELECTRICAL
  VALVE
  LEVEL
CONTROL
   oo
PURGE AIR
4    VENT
  ..
                                                            "-PURGE AIR ["[{"[--PURGE AIR[iT]*- PURGE AIR
                                     ii  ii
                                  , ,- ^
        I   ^   '':
AIR FL6wy*  ;;^
     	>•	
     P--1!- -,t --,r - 
-------
FRESH WATER
MAKE-UP
SPRAY—
    RECYCLE SUMP
                                                              MIST
                                                           ELIMINATOR
                                   DISTRIBUTION PLENUM.
                                                                     FILTER
                                                                               CORONA N0.2
 DUCT
HEATER
PURGE  AIR
INLET
                                                          ELEVATION VIEW
                                                         MIST ELIMINATOR
                                                          "PLAN VIEW"
                                      Fig. V-7.  Heated Purge Air System

-------
                              Section VI

              EXPERIMENTAL PROCEDURES AND TEST EQUIPMENT
The following table indicates the source test equipment used to measure
various parameters.  Further information concerning the UW Cascade
Impa'ctor is given below.
Table VI-1.  Particulate Source Test Parameters and Measurement Techniques.
                  Parameter
        Equipment
           1. Air

              a. Velocity and volume


              b. Temperature

              c. Moisture



           2. Water Spray Towers

              a. Water flow

           3. Aerosol

              a. Mass concentration


              b. Size distribution
S-type pitot tube with draft
gauge

Thermometer

Wet and dry bulb thermometer
and checked by volume of
condensate
Rotometers
UW Mark III and Mark V Cascade
Impactors

UW Mark III and Mark V Cascade
Impactors
The Mark III and Mark V Cascade Impactors were used to measure both
particle size distribution and mass concentration at both the inlet and
outlet test ducts respectively.  The impactors provide this information
by segregating the aerosol sample into discrete size intervals (seven
collection plates plus one final filter for Mark III and eleven col-
lection plates plus one final filter for Mark V).  The aerosol
                                   20

-------
weight on each plate provides size distribution information and the
total weight is used to determine the mass concentration.  The basic
components of a sampling train utilizing a UW Cascade Impactor are
shown schematically in Figure VI-1.  The impingers are used to collect
water vapor tn the sample air stream and provide a basis for calculat-
ing the moisture content of gas stream which may be checked against
the wet and dry bulb determination.  The dry gas meter is used to
determine isokinetic sampling conditions as well as the total  sample
volume.

By conducting simultaneous particle size distribution tests at both
the inlet and outlet test ducts, the size-dependent collection effi-
ciency curve of the pilot plant may be measured.

Overall efficiency measurements were also performed using in-stack
filters simultaneously at the inlet and outlet of the scrubber.
These measurements were performed per EPA Method 17 using a 3.54 in.
filter at the scrubber inlet and a 1.85 in. filter at the scrubber
outlet.  Reeve Angel  pre-washed glass fiber filters were used  to
minimize any SCL reaction with the filter material.
                                21

-------
GAS I
FLOW
TEST  DUCT
               IMPACTOR
           1/2  f> STEEL
           PIPE PROBE
                                 COURSE ADJUST
                                     VALVE
              VACUUM
              HOSES
                                  VACUUM
                                  GAUGE


* •
• 0
0
/
f^

-
X

r
4
" .
3.

' /
I
• «••«•
» * •
*

•\j


/
=^

» *
-••
e
9


[
• a • « •
o a
/ /
Y^
3
• *
0
1
; O
r
' /'
I
• * • •
•400*
0 °
u
/
^
1 	
'•'
t
f
   7
IMPINGER
                                     KNOCK
                                      OUT
FINE ADJUST THERMOMETERS
  VALVE
                                                       AIR TIGHT
                                                         PUMP
                                                       DRY  GAS
                                                         METER
                    ICE BOTTLE BATH
                 Fig. VI-1. UW Cascade Impactor Sampling Train

-------
                           Section VII

            PARTICIPATE COLLECTION EFFICIENCY RESULTS
A.  General Test Description

    Participate collection efficiency measurements on the U of W Electro-
    static Spray Scrubber were performed with the unit in two basMc
    operating modes.  In the first mode (two stage),  two particl^  charg-
    ing corona sections and two spray towers were used.   The components
    were connected in series (corona #1, spray tower  #1, corona #2, spray
    tower #2) followed by an electrostatic mist eliminator.  In the
    second mode (one stage), only one corona section  and one spray tower
    were on.  Water flow and high voltage power to corona #1 and spray
    tower #1 were turned off and they were utilized as ducting only.
    Scrubber operating parameters (SCA, L/G, gas residence time, no.  of
    components, etc.) were subsequently reduced.  Simultaneous cascade
    impactor measurements and in-stack filter tests,  described in  Section
    VI, were performed on the scrubber in both operating modes.


B.  Particulate Collection Efficiency (Two Stage Mode)

    1.   Cascade Impactor Measurements

        Initial cascade impactor tests were performed with the scrubber
        in the two stage mode.   Results of simultaneous  inlet/outlet
        impactor tests 3-8 are shown in Table VII-1.   Scrubber operating
        parameters (corona voltage,  mist eliminator voltage, and liquor
        flow rate) were held constant for all  tests with a variation  in
        spray voltage from 0 to 10 KV.   A significant variation in inlet
        gas flow from 919 scfm (1179 acfm) to 1244 scfm  (1515 acfm) was
        noted.   This variation was unavoidable.   With both the scrubber
        I.D,  fan and the booster fan operating at full  capacity, a
        variation in the negative static pressure at  the outlet of the
        air preheater (due to varying boiler conditions)  resulted  in
        subsequent variations in inlet gas flow.   This created changes
        in the parameters L/G,  SCA,  and gas residence time.   The levels
        of these parameters for impactor tests 3-8 are shown in page  2
        of Table VIM.   A variation in inlet gas temperature (measured
        downstream of the cooling tower)  from 133°F to 154°F was also
        noted.   Overall  particle collection efficiency for these tests
        ranged  from 99.30% to 99.89% (0.11% to 0.70%  penetration).  The
        particle collection efficiency and penetration as  a function  of
        particle size (aerodynamic  cut diameter  of cascade impactor
        stages, d5g)  for tests  3-8 are  shown in  Figure VII-1,   The aero-
        dynamic cut diameter of the  impactor stages is defined as  the
        diameter of the  particle of  unit density collected with 50%
        efficiency and is calculated by
                                23

-------
Table VII-1.    Results of Cascade Impactor Tests 3 Through 8 at Centralia Power Plant
               (Two Stage System).
Test No./
Date
3
11/30/77
4
11/30/77
5
12/1/77
6
12/1/77
7
12/8/77
8
12/14/77
Inlet Gas
Flow
(SCFM)
1031
1055
1071
1244
919
1076
Particle Hass Cone.
(grains sdcf)
Inlet
0.25924
0.20721
0.37242
0.31301
0.53698
0.37494
Outlet
.00052
.00099
.00056
. 00068
.00039
.00029
Overall
Coll. Eff.
(*)
99.73
99.30
99.77
99.70
99.88
99.89
Penetration
(*)
0.27
0.70
0.23
0.30
0.12
0.11
Total Lfquor
Flow Rate
(gpm)
15.5
15.5
15.5
15.5
16.0
15.5
Corona Voltage
(KV)
41
68
68
68
68
68
68
*2
80
80
80
80
80
80
Spray Voltage
(KV)
11
0
0
2
2
10
0
n
0
0
2
2
10
0
SCA
(ftVscfm)
0.061
0.059
0.058
0.050
0.068
0.058
L/G
(Gal/1000 scf)
15.0
14.7
14.5
12.7
17.4
14.4
Gas Residence Time (sec.)
Corona
Section
1.82
1.78
1.76
1.51
2.05
1.75
Spray
Tower
13.99
13.67
13.46
11.59
15.69
13.40
Mist
El fminator
0.86
0.84
0.83
0.72
0.97
n.83

-------
   89.89
                            T T i r
   98.9
  89.0
  80.0
   0.0
          UW Electrostatic  Scrubber
            Centralia Power Plant
                Nov.-Dec. 1977
        Units
Overall Efficiency (%)

Overall Penetration (%)
SCA (ft2/scfm)
L/G (gal/1000 scf)
/
Symbol
CD
A
+
X

t
Test
No.
3
4
5
6
7
8
Overall
Eff.
99.73
99.30
99.77
99.70
99.88
99.89
Pen.
0.27
0.70
0.23
0.30
0.12
0.11
SCA
.061
.059
.058
.050
.068
.058
L/G
15.03
14.69
14.47
12.66
17.41
14.40
                                                                     10-2
                                                                     4  £
                                                                        0

                                                                     6  85
                                                                        O-
                                                                     f)  *- -^
                                                                     IOP
                                                                        O
                                                                        cr
                                                                        ILJ
     10"1      2        4    8  8 10°       2       4    6  8 ID1
             PflRTICLE flERODYNflMIC DIflMETER, D50(MICRONS)
                                                           6

                                                           8
                                                           02
                                                       22.50
Fig. VII-1.  Particle Collection  Efficiency  and  Penetration vs. Particle
             Size for  Impactor  Tests' 3-8 (Two Stage System)
                                  25

-------
                        = r
                          L
                           18y D
                              „
                     5o       CY:


    where y is the gas viscosity, Dj the jet diameter, ^50 the
    inertia! impaction parameter at 50% collection efficiency for
    particles of diameter d5Q, C the Cunningham correction factor,
    and Vj the gas velocity in the jet diameter.  The collection
    of particles of diameter less than 1.0 micron ranged from about
    90% to 99. 5% (1.5 to 10% penetration).  The particle mass con-
    centrations (grains/sdcf) less than the stated particle aero-
    dynamic diameter, den (microns), for these tests are shown in
    Figures VII-2 and VII-3.  The curves in these graphs illustrate
    the reduction in the particle mass concentration for a particular
    particle size range on going from the scrubber inlet to the
    outlet.

    The cumulative particle size distributions (log-normal approxi-
    mation) measured at the scrubber inlet and outlet are shown in
    Figures VII-4 and VII^5.  The particle mass mean diameter
    (particle diameter at which 50% of the particle mass is greater
    than this diameter, and at which 50% is less than this diameter)
    was in the 11.5 to 29.4 micron diameter range at the scrubber
    inlet and in the 0.27 to 1.07 micron dtameter range at the outlet.
    A good correlation existed between the actual particle size
    (as measured with the cascade impactors) and the straight line
    (log-normal) approximation, this analysis uses the log-normal
    approximation to the particle size distribution.

    Particle mass concentrations measured at the scrubber outlet
    ranged from .00029 gratns/sdcf to .0099 grains/sdcf.   Sample
    weights on the outlet impactor substrates were consequently
    quite low (,01 to .15 mg).  The difference between the parti cu-
    late grain loading at the scrubber inlet and outlet prevented
    simultaneous sampling.  Despite outlet sampling times as high
    as 1  hour, low weights were recorded.  Details on the sampling
    techniques (sampling  rates, nozzle sizes, types of substrates
    used, etc,) for both the impactor tests and the in-stack filter
    tests are listed in Appendix A.

2.  In-stack Filter Measurements

    Overall  particulate collection efficiency measurements using in-
    stack filters were also performed with the scrubber in the two
    stage mode.  The results of tests 1-F through 8-F are shown in
    Table VII-2.   The isokinetic sampling rate for the outlet filter
    was increased to collect a larger sample (80 to 100 acf).   All
    scrubber operating parameters were held constant  with the
    exception of spray voltage which was varied between 0 and 10 KV.
    Inlet conditions (mass concentration, gas flow, etc.)  did not
    vary as significantly as for impactor tests 3-8.   Overall  parti-
    culate collection efficiencies ranged from 99.77% (.23% penetra-

                             26

-------
         1.0
                                    1.0
10.0     20   30
                                                        100.0
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-------
0.1 1.0 10.0 20 30 100.0



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'. UW Electrostatic Scrubber
Centrali a Power Plant
Dec. 1977

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0.1 l".0 10.0 20 30 100.0
            Particle Aerodynamic Diameter, C^  (microns)
Fig.  VII-3.   Particle Mass Concentration  for  Particles  Less  Than
             Stated Diameter for Cascade  Impactor Tests 6-8.
                             28

-------
100.0
 80.0

 60.0
 50.0
 40.0

 30.0

 20.0
  10.0

   8.0

1 6<0
& 5.0
i4.0

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tit

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    .6
    .5

    .4

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    .2
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                                              I    I
UW Electrostatic Scrubber
  Centralia Power Plant
      Nov.-Dec. 1977
          Inlet Size
          Distribution
                                         '
                                                   /
                                   //   /
                                  ///
                                   /
                                                       
-------
100.'0
 80.0

 60.0
 50.0
 40.0

 30.0

 20.0
  10.0

  8.0

I 6'°
& 5.0

I 4.0

S 3.0
e-
tal
2
§2.0

bl
U
   .8

   .6
   .5

   .4

   .3

   .2
  0.1
 i  r
         r  i
UW Electrostatic Scrubber
  Centralia Power Plant
      Nov.-Dec. 1977
                  Inlet Size
                  Distribution
                                             /'

                                            /'    '
                                            /'    /
                              / 7
                                        /
                                        8
                                             / Outlet  Size
                                             /  Distribution
                                            1   1   I   L
     OCX
0.1  0.2 Q5 I  2    3   10   20 30 40 50 60 70 80   90  95
                                                                    99   99B 99.9  99.99
                      % of  MASS LESS   THAN  STATED  DIAMETER

        Figure VII-5.   Inlet and Outlet Particle Size Distribution for
                        Cascade  Impactor Tests 6-8  (Log-Normal  Approximation)
                                        30

-------
Table VII-2.   Results of Simultaneous In-stack Filter Tests 1-F Through  8-F  at  Centralia  Power Plant
              (Two Stage System).
Test No./
Date
1-F
1/24/78
2-F
1/24/78
3-F
1/24/78
4-F
1/24/78
-5-F
1/24/78
6-F
1/24/78
7-F
2/1/78
8-F
2/1/78
Inlet Gas
Flow
(scfm)
1072
1091
1061
1108
1146
1192
1182
1142
Particle Mass Cone.
(grains/sdcf )
Inlet
0.40634
0.39347
0.31080
0.37958
0.39473
0.45178
0.83886
0.63517
Outlet
.00052
.00067
.00030
. 00022
.00021
.00015
.00018
.00029
Overall
Coll. Eff.
(%)
99.85
99.77
99.88
99.99
99.94
99.96
99.96
99.93
Penetration
(«)
0.15
.23
.12
.01
.06
.04
.04
.07
Total Liquor
Flow Rate
(gpm)
17.5
18.5
17.5
17.5
17.5
16.1
17.0
17.0
Corona Voltage
(KV)
#1
68
68
68
68
68
68
68
68
12
80
80
80
80
80
80
80
80
Spray Voltage
(KV)
#1
0
0
0
5
5
10
0
10
#2
0
0
0
5
5
10
0
10
SCA
(ft2/ scfm)
.058
.057
.059
.056
.055
.052
.053
.055
L/G
(Gal/1000 scf)
16.32
16.96
16.49
15.79
15.70
13.51
14.38
14.98
Gas Residence Tine (sec.)
Corona
Section
1.75
1.72
1.77
1.70
1.64
1.58
1.59
1.65
Spray
Tower
13.45
13.22
13.59
13.01
12.58
12.10
12.20
12.63
Mist
Eliminator
0.83
0.82
0.84
0.80
0.78
0.75
0.75
0.78

-------
        tion) with no charge on the sprays to 99.99% (.01  penetration)
        with 5 KV(+) charge on the sprays.  A direct correlation between
        particle collection efficiency and spray voltage was not apparent
        although the 3 tests exhibiting the highest overall  participate
        collection efficiencies were either a 5 KV(+) or 10  KV(+) charge
        on the sprays.  The outlet particle mass concentrations measured
        ranged from 0.00018 to 0.00067 grains/sdcf.   Simultaneous sampling
        at the inlet and outlet of the scrubber was not possible for
        either the in-stack filter tests or the impactor tests due to
        the extreme difference between inlet and outlet mass concentra-
        tions in this operating mode.


C.  Particulate Collection Efficiency (One Stage Mode)

    1.  General System Description

        Operation of the scrubber in the one stage mode involves utiliza-
        tion of corona #2 and spray tower #2 only.  With corona #1  and
        spray tower #1 inactive, the active length (in  the direction of
        gas flow), of particle charging section and spray tower section
        is reduced 50% and 29% respectively.   Gas residence  time in the
        combined active sections is subsequently reduced 32%.   The gas
        cooling tower and the electrostatic mist eliminator  were used
        in both the one and two stage modes.   Inlet volumetric gas flow
        rate remained approximately the same as measured for the two
        stage tests.   Total liquor flow to the spray sections  was reduced
        to approximately 12.0 gpm resulting in a reduction in  liquor to
        gas flow rate ratio of about 27%.

    2,  In-stack Filter Measurements

        Overall  particle collection efficiency measurements  (in-stack
        filter tests) were initially performed on the one  stage system.
        The results of tests 9-F through 16-F are shown in Table VII-3.
        Overall  collection efficiency ranged  from 99.77% to  99.89%
        (0.23% to 0.11% penetration).   Particle mass concentration
        measured at the scrubber inlet ranged from 0.6774  to 1.1390
        grains/sdcf while outlet particle  mass concentrations  varied
        from 0,00077  to 0.00116 grains/sdcf.   Despite the  reduction in
        the operating parameters previously described,  outlet  particle
        mass concentrations remained low,  resulting  in  extended sampling
        time and low outlet sample weights.   No direct  correlation
        between spray voltage and particle collection efficiency was
        noted.   Such a correlation is  difficult to establish when the
        low outlet sample weights introduced  a significant probable
        error associated with weighing.   In addition to weighing related
        errors,  there are other probable errors inherent in  the sampling
        process.   The difference in inlet  and outlet sampling  times
        necessitated  by the difference in  mass concentration also had
        a  possible effect upon the results.   During  the outlet testing
        period (up to 60 min.), system upsets and perturbations could
        affect the outlet sample and not be accounted for  by the inlet
        (10 minute) sample.
                                 32

-------
         Table VII-3.  Results of Simultaneous In-stack Filter Tests 9-F Through 16-F at Centralia Power  Plant
                       (One Stage System).
Test No./
Date
9-F
2/2/78
10-F
2/2/78
11-F
2/2/78
12-F
2/2/78
13-F
2/2/78
14-F
2/3/78
15-F
2/3/78
16-F
2/3/78
Inlet Gas
Flow
(scfm)
1279
1122
1179
1253
1210
1141
1190
1173
Particle Mass Cone.
(grains/sdcf)
Inlet
1.1390
0.8584
0.6774
0.6920
0.7530
0.7650
0.7110
0.7030
Outlet
.00095
.00116
.00077
.00088
.00101
.00115
.00085
.00113
Overall
Coll. Eff.
(X)
99.89
99.80
99.84
99.82
99.82
99.79
99.83
99.77
Penetration
(%)
.11
.20
.16
.18-
.18
.21
.17
.23
Total Liquor
Flow Rate
(gpm)
12.5
12.5
12.0
12.0
12.0
12.5
12.5
12.0
Corona Voltage
(KV)
#1
..
—
.-
—
__
--
._
--
#2
80
80
80
80
80
80
80
80
Spray Voltage
(KV)
#1
—
..
..
__
__
.-
..
--
12
0
2
5
10
0
5
2
10
§W
(ftz/scfm)
.024
.028
.027
.025
.026
.027
.026
.027
L/G
(Gal/1000 scf)
9.77
11.14
10.18
9.58
9.92
10.96
10.50
10.23
Gas Residence Time (sec.)
Corona
Section
0.74
0.84
0.80
0.75
0.73
0.82
0.79
0.80
Spray
Tower
7.96
9.07
8.63
8.12
8.41
8.92
8.55
8.68
Hist
Eliminator
0.70
0.79
0.75
0.71
0.74
0.78
0.75
0.76
CO
CO

-------
                   Table VII-4.  Results of Simultaneous Impactor Tests 12-18, Centralia Power Plant
                                 (One Pass System).
Test No./
Date
12
2/8/78
13
2/8/78
14
2/8/78
15
2/8/78
16
2/9/78
17
2/9/78
18
2/9/78
Inlet Gas
Flow
(scfm)
1026
1066
982
970
1025
855
1142
Particle Mass Cone.
(grains/sdcf)
Inlet
.33605
.57211
.26609
.20468
.22907
.42355
.48158
Outlet
.00060
.00071
.00088
.00045
.00047
.00042
.00081
Overall
Coll. Eff.
W
99.73
99.83
99.50
99.65
99.70
99.84
99.77
Penetration
(%)
.27
.17
.50
.35
.30
.16
.23
Total Liquor
Flow Rate
(9pm)
12.5
12.0
12.0
12.5
12.0
12.0
12.0
Corona Voltage
(KV)
11
--
--
--
--
--
--
--
n
80
80
80
80
80
80
80
Spray Voltage
(KV)
*1
--
--
--
--
--
--
--
#2
0
2
2
0
0
0
10
SCA
(ftVscfm)
.030
.029
.032
.032
.031
.037
.027
L/G
(Gal /1 000 scf)
12.18
11.26
12.22
12.89
11.71
14.04
10.51
Gas Residence Time (sec.)
Corona
Section
0.92
0.88
0.96
0.97
0.92
1.10
0.82
Spray
Tower
9.92
9.55
10.37
10.49
9.93
11.91
8.91
Hist
Eliminator
0.87
0.83
0.91
0.92
0.87
1.04
0.78
OJ

-------
   99.99
£ 99.9

UJ


UJ
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         UW  Electrostatic  Scrubber
           Centralia  Power Plant
                  Feb.  1978

                    Units
            Overall Efficiency (%)

            Overall Penetration  (%)

            SCA (ft2/scfm)

            L/G (gal/1000 scf)
0.0  L_
  10-1
/
Symbol
O
A
4-
X
<1>
*
X
Test
No.
12
13
14
15
16
17
18
Overall
Eff .
99.73
99.83
99.50
99.65
99.70
99.84
99.77
Pen,
0.27
0.17
0.50
0.35
0.30
0.16
0.23
SCA
.030
.029
.032
.032
.031
.037
.027
L/G
12.18
11.26
12.22
12.89
11.71
14.04
10.51
                                                                     10
                                                                       .-2
                                                                      4  LJ

                                                                      6  UJ

                                                                      8  —
                                                                         z
                                                                         o
                                                                         cc
                                                                         a:
                                                                         UJ
                                                                         UJ
                                                                         o_
              2       4   6   8  10°      2       4   6   8  Id1
              PRRTICLE RERODYNflMIC DIRMETER,  D50(MICRONS)
2 2
                                                                      6

                                                                      8
                                                                     102
                                                                     50
      Fig. VII-6.   Particle Collection Efficiency and Penetration vs.
                    Particle Size for Impactor Tests 12-18 (One Stage  System)
                                 •35

-------
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                                                       "T
                                                                    IIII1Ti
             UW Electrostatic Scrubber
               Centralia Power Plant
                    Feb. 1978
                                    Inlet
                                    Tests
Q  Test 12

-I-  Test 13

    Test 14

 X  Test 15
                                                           -£>

                                                            Outlet
                                                            Tests
                             i  i
                                                                   j—i	i
         0.1
                         1.0                     10.0

               Particle Aerodynamic  Diameter,  d50 (microns)
                      100.0
         Fig.  VII-7.   Particle'Mass Concentration for Particles Less Than
                      Stated Diameter for Cascade Impactor Tests  12-15.

                                     36

-------
      1.0
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             UW Electrostatic  Scrubber
               Centralia  Power Plant
                    Feb.  1978
                                                                       Inlet
                                                                       Tests
                                                            O  Test  16

                                                            4-  Test  17

                                                            X  Test  18
                                                                   Outlet
                                                                   Tests
                                                    i  i i
                                                                    j _ i
          0.1
                                1.0                     10.0  20.0 30.0

                      Particle Aerodynamic Diameter, 
-------
    Comparing the composite results of the two stage and one stage
    systems, the decrease in certain operating parameters as previously
    discussed has only a slight affect on the overall  particle collec-
    tion efficiency of the system.   The average overall  particle col-
    lection efficiency of the two stage system (tests  1-F through 8-F)
    is 99.93% (0.07 penetration).  The results of tests  9-F through
    15-F (one stage system) show an average overall  particle collec-
    tion efficiency of 99.825% (0.18% penetration).

3.  Cascade Impactor Measurements

    Particle collection efficiency  measurements using  cascade impactors
    were also performed with the scrubber operating  in the one stage
    mode.   The results of these tests are shown in Table VII-4.   Over-
    all  particle collection efficiency ranged from 99.50% to 99.84%
    (0.16% to 0.50% penetration).   Particle mass concentration measured
    at the scrubber inlet varied from 0.30458 to 0.57211  grains/sdcf
    while outlet concentrations ranged from 0.00042  to 0.00088 grains/
    sdcf.   Particle collection efficiency as a function  of particle
    size for these tests is illustrated in Figure VII-6.   The collec-
    tion efficiency for particles smaller than 1.0 micron in diameter
    ranged from about 83% to 99%.  Figures VII-7 and VII-8 illustrate
    the  particle mass concentration (grains/sdcf) less than stated
    particle diameter (microns) for the cascade impactor tests on the
    one  stage system.   Relative particulate concentrations (grains/
    sdcf)  measured at the scrubber  inlet and outlet  for  a particular
    size range can be directly obtained from these curves.   The  cumu-
    lative particle size distributions (log-normal approximations)
    measured at the scrubber inlet  and outlet for impactor tests 12-18
    are  shown in Figures VII-9 and  VII-10.   Mass mean  diameter (dso)
    ranged from 23.13 to 76.5 microns at scrubber inlet  and from
    0.0324 to 1.032 microns at the  scrubber outlet.

    A comparison of the particle collection efficiency as a function of
    particle size between the two stage and one stage  system is  shown in
    Table VII-5.  The incremental particle collection  efficiencies are shown
    in the mean values for all  the  cascade impactor  tests performed in either
    the  one stage or two stage modes.   The particle  diameter is  repre-
    sented by the midpoint of the increment.   The reduction of certain
    operating parameters (SCA,  L/G,  gas residence time)  on changing from
    the  two stage to one stage mode resulted in an increase, in the
    particle penetration from 3.35% to 7.29% at 0.4  microns diameter and
    from 0.76 to 1.4% at 1.2 microns diameter.   In general  the particle
    penetration for these submicron particle sizes doubled on going from
    two  stage to one stage operation.
                              38

-------
100.0

 80.0

 60.0
 50.0

 40.0

 30.0


 20.0
  10.0

  8.0


I 6-°
§ 5.0

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£ 3.0


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I
    .8

    .6
    .5

    .4

    .3


    .2
           UW Electrostatic Scrubber
             Centralia Power Plant
                  Feb. 1978
                Inlet Size
                Distributions
                     14 15
                           12
                                                            I
                                                            I
 /     y
 /     '
/    '
   /
                                                      //•  //
                                                    / /   /Outlet Size
                                                   / /    V  Distributions
                                              ,   if  i
                                             / /   /
                                               /   i
                                            'I      I
                                                15
   0.1
     00*
           O.I 0.2 09 I   2
                               10   20 30 40 50 60 70 80  90  95
    99   99B 99.9  99.99
                      %  Of  MASS LESS  THAN  STATED  DIAMETER


        Figure VII-9.  Inlet and Outlet Particle Size Distributions for Cascade
                       Impactor Tests 12-15  (Log-Normal  Approximation)
                                        39

-------
100.0
 80.0

 60.0
 50.0
 40.0

 30.0

 20.0
  10.0

  8.0

| 6.0
I 5.0

I 4.0

5 3.0
>-
Ul

I 2.0

u
_!
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    .5

    .4

    .3

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   0.1
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                                         I     I   I
UW Electrostatic Scrubber
  Centralia Power Plant
       Feb. 1978
  Inlet Size
  Distributions,
    18    16   17
            J	I
                  I  i   i
                 /   x/
             - /    //  Outlet Size
             /    //   Distributions
                        /
                       18
       I/
          16
      0.01   0.1 0.2 Q5  I  2
                   10
20 30 40 50 60 70 80   90  95
99   99B 99.9  9999
                       %  Of  MASS  LESS   THAN  STATED  DIAMETER

       Figure VII-10.   Inlet  and  Outlet  Particle  Size  Distributions for
                        Cascade  Impactor  Tests  16-18  (Log-Normal  Approximation)
                                      40

-------
      Table VII-5  Comparison of Particle Collection Efficiencies
                   Between the Two Stage and One Stage System
Particle
Diameter
(microns)
0.4
0.5
0.6
0.75
0.95
1.20
Two Stage
Coll. Eff.
(«).
96.65
97.60
98.13
98.60
98.97
99.24
Penetration
(o/\
\h]
3.35
2.40
1.87
1.40
1.03
0.76
One Stage
Coll. Eff.
(%)
92.71
94.76
96.02
97.17
98.04
98.60
Penetration
(%)
7.29
5.24
3.98
2.83
1.96
1.40
4.  Integrating Nephelometer Measurements

    An integrating nephelometer was used to measure the light scat-
    tering coefficient at the scrubber outlet where the particle mass
    concentration was typically 0.0004 to 0.0015 grains/sdcf.   A sample
    gas volume was extracted from the outlet test port through a heated
    probe (to prevent condensation) and into the nephelometer.   The
    single wavelength (530 nm)  nephelometer is an .instrument which meas-
    ures the scattering portion of the extinction coefficient due to
    particles in the sample gas.   It provides an instantaneous, continu-
    ous readout of the coefficient Bscat (M-l) which is a  direct indi-
    cation of particle concentration, particularly in the  0.1  to 1.0
    micron size range.  The nephelometer was originally designed for
    atmospheric measurements and is consequently sensitive to extremely
    low particle concentrations.   Since no means of monitoring  the inlet
    particle mass concentrations was available, the results of  this test
    provide only a relative measurement of particle mass concentration
    at the scrubber outlet with variations in spray voltage.

    For this test the scrubber  was operated in the one stage mode with
    the voltage to corona #2 at 80 KV(-), mist eliminator  voltage at
    60 KV (+) and liquor flow rate at 12 gpm.   The voltage to the liquor
    sprays was held at 0, 2, 5, 10, 15, and 20 KV with 5 minute time
    intervals for each voltage  setting.  During this time  period the
    light scattering coefficient, Bscat> was measured using the inte-
    grating nephelometer.   The light scattering measurement results
    of this test are presented  in Figure VII-11.
                               41

-------
               2.24 -
                2.0
                1.75 -
   cscat
   (M'1)
ro
                1.50-
                1.25  -
                1.0
                                         (Spray Voltage)
                                           (20 KV)    '  (0 KV)
                      (0 KV)  (2 KV)   ,  (5 KV)
                     Figure VII-11.
                       Time (min.)

Light Scattering Coefficient,  Bsca^, Measured  at  the Outlet of  the UW
Electrostatic Spray Scrubber for  Various  Spray Voltages  (All Other
Parameters Held Constant)

-------
                             Section VIII

                              REFERENCES
1.  Kraemer, H. F. and H. F. Johnstone  (1955) "Collection of aerosol
         particles in the presence of electric fields,"  Ind. Engr.
         Chem. 47_ 2426.

2.  Penney, G. W. (1944) "Electrified liquid spray dust  precipitatpr,"
         U.S. Patent No. 2,357,354.

3.  Pilat, M. J., S. A. Jaasund, and L. E. Sparks (1974) "Collection
         of aerosol particles by electrostatic droplet spray scrubbers,"
         Envir. Sci. & Tech. 8_ 340-348.

4.  Pilat, M. J. (1975) "Collection of  aerosol particles by electro-
         static droplet spray scrubber," APCA Journal 25_ 176-178.

5.  Pilat, M. J. and D. F. Meyer (1976) "University of Washington
         electrostatic spray scrubber evaluation"  Final Report on
         Grant No. R-803278, EPA Report No. EPA-600/2-76-100 (NTIS
         No. PB 252653/AS).

6.  Pilat, M. J., G. A. Raemhild, and A. Prem (1978) "University of
         Washington electrostatic scrubber tests at a steel plant,"
         EPA Report No. EPA-600/7-78-177a.
                                     43

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          APPENDIX A





Details on Sampling Techniques
                44

-------
Sampling Details
Test Sequence
Type of Test
Collector Used
Type of
Substrate
Sampling
Nozzle Dia.
Samp! ing
Time
Gas Volume
Sampled
(acf)
Inlet
Outlet
Inlet
Outlet
Inlet
Outlet
Inlet
Outlet
Inlet
Outlet
3-8
Simultaneous
Cascade Impactor
11 stage MK5
Cascade Impactor
7 stage MK3
Cascade Impactor
Ungreased, s.s.
Impaction Insert
Ungreased, s.s.
Impaction Insert
3/16 in.
1/4 in.
8-15 min.
18-60 min.
2.8-3.5
13.4-66.4
IF - 8F
Simultaneous
In-Stack Filter
90 mm
Filter
47 mm
Filter
Reeve Angel
934AH Filter
Reeve Angel
934AH Filter
3/16 in.
1/4 in.
10 min.
40 min.
1.8-3.0
60.5-113.5
9F - 16F
Simultaneous
In-Stack Filter
90 mm
Filter
47 mm
Filter
Reeve Angel
934 AH" Filter
Reeve Angel
934AH Filter
3/16 in.
1/4 in.
10 min.
40 min.
2.8-3.5
88.3-111.3
12 - 18
Simultaneous
Cascade Impactor
11 Stage MK5
Cascade Impactor
7 stage MK3
Cascade Impactor
Ungreased, s.s.
Impaction Insert
Ungreased, s.s.
Impaction Insert
3/16 in.
1/4 in.
20 min.
60 min.
5.0-7.16
80.5-95.4

-------
          APPENDIX B
Converting Units of Measure
                46

-------
                         Appendix B
                CONVERTING UNITS OF MEASURE
Environmental Portection Agency policy is to express all measure-
ments in Agency documents in metric units.  In this report, however,
to avoid undue costs or lack of clarity, English units are used
throughout.  Conversion factors from English to metric units are
given below.
     \
To convert from
pounds
To
Multiply by
f
feet
inches
BTU
BTU/lb
acfm
gpm
grains/sdcf
f2scfm
Kg
dynes /cm2
n,2
m3
meters
meters
joules
joules/gm
acm/hr
1/m
gm/sdcm
2
m scm/hr
°C
0.45359
+14.7 x 68947.6
0.0929
0.028317
0.3048
0.0254
1054.35
2.235
1.699
3.79
2.29
0.0547
5/9
                              47

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                                 TECHNICAL REPORT DATA
                          (Please read Instructions on the reverse before completing}
 1. REPORT NO.
 EPA-600/7-78-177b
     2.
                                                       3. RECIPIENT'S ACCESSION-NO.
 4. TITLE AND SUBTITLE
 University of Washington Electrostatic Scrubber Tests
    at a Coal-fired Power Plant
                                5. REPORT DATE
                                 December 1978
                                6. PERFORMING ORGANIZATION CODE
 7. AUTHOR(S)
                                                      8. PERFORMING ORGANIZATION REPORT NO.
 M.J. PilatandG.A. Raemhild
 9. PERFORMING ORGANIZATION NAME AND ADDRESS
 University of Washington
 Department of Civil Engineering
 Seattle, Washington  98195
                                10. PROGRAM ELEMENT NO.
                                E HE 62 4 A
                                11. CONTRACT/GRANT NO.

                                Grant R804393
 12. SPONSORING AGENCY NAME AND ADDRESS
 EPA, Office of Research and Development
 Industrial Environmental Research Laboratory
 Research Triangle Park, NC  27711
                                13. TYPE OF REPORT AND PERIOD COVERED
                                Final; 6/77 - 10/78	
                                14. SPONSORING AGENCY CODE
                                  EPA/600/13
 IB. SUPPLEMENTARY NOTES T£RL-RTP project officer is Dale L.
 541-2925.
                                  Harmon, Mail Drop 61, 919/
 16. ABSTRACT
          The report gives results of tests of a 1700 cu m/hr University of Washing-
 ton Electrostatic Spray Scrubber pilot plant on a coal-fired boiler to demonstrate
 its effectiveness for controlling fine particle emissions. The multiple-pass,  portable
 pilot plant combines oppositely charged aerosol  particles and water droplets  in two
 water spray towers. Aerosol negative-charging  sections precede each,spray  tower.
 The scrubber was tested in two modes: two-stage, including two active; particle
 charging corona sections and two spray towers;  and single-stage, including only one
 corona section and one spray tower. Simultaneous inlet and outlet source  tests pro-
 vided both size-dependent and overall mass basis particle collection efficiency in-
 formation. Measured overall particle collection efficiencies ranged from 99. 30 to
 99.99%, depending on scrubber operating conditions ,  inlet particle size distribution,
 and mass  concentration. Particle mass concentrations measured at the scrubber
 outlet ranged from 0.00041 to 0.0027 g/cu m. The average overall particle collection
 efficiency for all tests performed in the two-stage mode was 99. 93%; single-stage
 average efficiency was  99. 83%.
 7.
                             KEY WORDS AND DOCUMENT ANALYSIS
                DESCRIPTORS
                    b.IDENTIFIERS/OPEN ENDED TERMS  C.  COS AT I Field/Group
 Pollution
 Gas Scrubbing
 Scrubbers
 Electrostatics
 Coal
 Combustion
Dust
Aerosols
Pollution Control
Stationary Sources
Particulate
University of Washing-
 ton Scrubber
13B
07A,13H
131
20C
2 ID
21B
11G
07D
 I. DISTRIBUTION STATEMENT
 Unlimited
                                          19. SECURITY CLASS (This Report)
                                           Unclassified
                                             21. NO. OF PAGES

                                                   58
                    20. SECURITY CLASS (This page)
                    Unclassified
                                                                   22. PRICE
EPA Form 2220-1 (9-73)
                                        48

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