MONITORING TO DETECT
PREVIOUSLY UNRECOGNIZED POLLUTANTS
IN SURFACE WATERS
APPENDIX
JULY 1977
U.S. ENVIRONMENTAL PROTECTION AGENCY
OFFICE OF TOXIC SUBSTANCES
WASHINGTON, D.C. 20460
-------
77-
TtCHNiCAL REPORT DATA
ji1 rcnJ Iinojiictiotis on the reverse before completing)
\. REPORT NO.
EPA-560/7-77-001a
4. TITLE AND SUBTi TLE
Monitoring to Detect Previously Unrecognized
Pollutants in Surface WatersAppendix: Organic
Analysis Data
7. AUTHORtS)
B. B. Ewing, E.S.K. Chi an, J. C. Cook, C. A. Evans,
P. K. Hopke, E. G. Perkins, and J. C. Means
9. PERFORMING ORGANIZATION NAMF AND ADDRESS
Institute for Environmental Studies
408 S. Goodwin Avenue
University of Illinois at Urbana-Champaign
Urbana, Illinois 61801
3. RECIPIENT'S ACCESSION-NO.
5. REPORT DATE
July 1977
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO.
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
EPA 68-01-3234
12. SPONSORING AGENCY NAME AND ADDRESS
United States Environmental
Office of Toxic Substances
Washington, D. C. 20460
Protection Agency
13. TYPE OF REPORT AND PERIOD COVERED
Appendix to final report.
14. SPONSORING AGENCY CODE
15. SUPPLEMENTARY NOTES
16. ABSTRACT
Samples of surface waters were collected from 204 sites near heavily industrialized
areas across the United States. The samples were analyzed for all contaminants
present at concentrations greater than one part per billion. Each water sample
was preconcentrated for analysis of organics in three fractions: volatile
organics by nitrogen-gas stripping and the less-volatile organics by extraction
with chloroform under both basic and acidic conditions. Organic constituents
were identified by gas chromatography/mass spectrometry and quantified by gas-
chromatographic techniques. Inorganic constituents were determined by spark-
source mass spectrometry, energy-dispersive x-ray fluorescence analysis, and
instrumental neutron activation analysis. For comparison with previous data from
the same sites, the samples were also analyzed for total chemical oxygen demand,
turbidity, conductivity, pH, color, oxidation-reduction potential, suspended
solids, and volatile suspended solids. Results of the inorganic analyses were
presented in previous quarterly progress reports. Final results of the organic
analyses are presented in this appendix to the final report.
17.
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
Water quality
Water pollution
Water analysis
Water chemistry
Surface waters
b.IDENTIFIERS/OPEN ENDED TERMS
Trace contaminants
Organic compounds
Volatile organic
compounds
Industrial pollution
Nationwide survey
c. COSATi l-'icld/Group
8h
7b, 7c, 7e
13. DISTRIBUTION1 STATEMENT
Unrestricted
Available from National Technical Infor-
mation Service. Springfield. VA 22151
19. SECURITY CLASS (This Report)
U nclassified
25. SECURITY CLASS (This page)
Unclassified
21. NO. OF PAGES
4
22. PRICE
EPA Form 2220-1 (9-73)
-------
EPA-560/7-77-001a
MONITORING TO DETECT PREVIOUSLY UNRECOGNIZED
POLLUTANTS IN SURFACE WATERS
APPENDIX: ORGANIC ANALYSIS DATA
INSTITUTE FOR ENVIRONMENTAL STUDIES
University of Illinois at Urbana-Champaign
B. B. Ewing
E. S. K. Chian
J. C. Cook
F. B. DeWalle
C. A. Evans
P. K. Hopke
J. H. Kim
Principal
Investigators
J. C. Means
R. Mil berg
E. G. Perkins
J. D. Sherwood
W. H. Wadlin
Final Report
Contract No. 68-01-3234
July 1977
Project OfficerVincent J. DeCarlo
Prepared for
Office of Toxic Substances
U.S. Environmental Protection Agency
Washington, D.C. 20460
Document is available to the public through the National Technical Information
Service, Springfield, Virginia 22151
-------
NOTICE
This report has been reviewed by the Office of Toxic Substances, EPA,
and approved for publication. Approval does not signify that the contents
necessarily reflect the views and policies of the Environmental Protection
Agency, nor does mention of trade names or commercial products constitute
endorsement or recommendation for use.
-------
1
TABLE Bl
Organic Compounds Identified in Sample
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
Volatile Compounds
Dichloromethane
Acetone
Chloroform
Trichloro-trifluoroethane
Trichloroethylene
Benzene
Tetrachloroethyl ene
Toluene
Approximate
Level (PPB)
1
2
30
5
4
3
2
2
-------
TABLE B2
Organic Compounds Identified in Sample # 1A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
Relative
Retention
Time
0.435
0.780
0.792
0.826
0.893
0.926
0.954
0.978
1.000
1.049
1.061
1.088
1.095
1.131
1.143
1.186
1.216
1.232
1.265
1.323
1.348
1.366
1.388
1.403
1.418
1.451
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C = 12
Methyl Trichlorophenyl Ether
Methyl Tetrachlorophenyl Ether
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Fatty Acid Methyl Ester C > 15
+ Methyl Pentachlorophenyl Ether
Fatty Acid Methyl Ester C >_ 15
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Dibutyl Phthalate
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 19
Fatty Acid Methyl Ester C >_ 20
?
Fatty Acid Methyl Ester C ^ 22
Fatty Acid Methyl Ester C >_ 22
Di ethyl Hexyl Phthalate
?
?
C,c - Terpineol
?
Fatty Acid Methyl Ester C > 26
?
Approximate
Level (PPB)
_ _ _
10
1
5
9
12
8 (mix)
2
45
4
4
14
43
4
4
11
35
6
15
14
14
7
6
7
2
4
-------
TABLE B3
Organic Compounds Identified in Sample #1B
Relative
Retention
Peak # Time
1
2
3
4
5
6
Compounds in Base Extract
Xylene
Dibromo-chl oroethane
Camphor (IS)
Diisobutyl Phthalate
Dibutyl Phthalate
Terpineol
Approximate
Level (PPB)
19
14
1
1
1
TABLE B4
Organic Compounds Identified in Sample # 2S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
Volatile Compounds
Acetone
Chloroform
Trichloro-trifluoroethane
Trichloroethane
Bromo-dichloromethane
Trichloroethylene
Benzene
Di bromo-chl oromethane
Tetrachloroethylene
Fluoro-dichloro-bromomethane
Toluene
Approximate
Level (PPB)
2
5
2
1
9
2
4
2
1
1
2
-------
TABLE B5
Organic Compounds Identified in Sample # 2A
Peak #
1
2
3
4
5
6
Relative
Retention
Time
0.467
0.899
1.000
1.105
1.319
1.386
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
2
4
2
1
1
TABLE B6
Organic Compounds Identified in Sample #2B
Peak #
1
2
3
4
Relative
Retention
Time
Compounds in Base Extract
Tetrachloroethane
1 ,2-Diethoxyethane
Camphor (IS)
Terpineol
Approximate
Level (PPB)
2
2
2
-------
TABLE B7
Organic Compounds Identified in Sample #3S
Peak #
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time Volatile Compounds
Dichloromethane
Acetone
Trichloro-fluoromethane
Chloroform
Trifluoro-trichloroethane
Butane
Trichloroethylene
Benzene
Tetrachloroethylene
Toluene
Chlorobenzene
Approximate
Level (PPB)
1
3
6
8
3
6
4
2
1
1
1
-------
TABLE B8
Organic Compounds Identified in Sample # 3A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Peak i
1
2
3
4
5
Relative
Retention
Time
0.519
1.000
1.055
1.085
1.091
1.131
1.167
1.179
1.213
1.262
1.319
1.349
1.365
1.402
Organic
Relative
Retention
Time
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Dibutyl Phthalate
Methyl Stearate
?
?
Fatty Acid Methyl Ester C i 20
?
?
Diethyl Hexyl Phthalate
?
?
?
TABLE B9
Compounds Identified in Sample #3B
Compounds in Base Extract
Tetrachl oroethyl ene
Diethoxyethane
Dichlorobenzene
Camphor (IS)
?
Approximate
Level (PPB)
3
3
1
3
2
1
2
9
2
6
2
3
3
Approximate
Level (PPB)
2
3
4
1
-------
TABLE BIO
Organic Compounds Identified in Sample # 4S
Peak 1
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time Volatile Compounds
Dichloromethane
Acetone
Trichlorofluoromethane
Chloroform
Trichloro-trifluoroethane
Pentane
Trichloroethane
Trichloroethylene
Benzene
Tetrachloroethylene
Toluene
Approximate
Level (PPB)
2
3
6
9
3
2
1
2
1
1
1
TABLE Bll
Organic Compounds Identified in Sample # 4A
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
Sample 4A was destroyed and no quantitative data or
chromatogram is available.
-------
8
TABLE B12
Organic Compounds Identified in Sample # 4B
Peak #
1
2
3
4
5
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time Compounds in Base Extract
Tetrachloroethylene
Camphor (IS)
Naphthalene (IS)
Unidentified Phthalate
Terpineol
TABLE B13
Organic Compounds Identified in Sample # 5S
Relative
Retention
Time Volatile Compounds
Dichloromethane
Acetone
Tetrahydrofuran
Chloroform
Trifluoro-trichloroethane
Trichloroethane
Trichloroethylene
Benzene
Hexane
Tetrachloroethylene
Toluene
Chlorobenzene
Approximate
Level (PPB)
11.3
3
1
Approximate
Level (PPB)
2
2
1
100
1
1
6
2
1
4
1
1
-------
TABLE B14
Organic Compounds Identified in Sample # 5A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Relative
Retention
Time
0.444
0.559
0.894
0.927
0.951
1.000
1.036
1.058
1.097
1.182
1.219
1.265
1.326
1.349
1.365
1.386
1.402
1.419
1.453
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Camphor
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
Hydrocarbon C ^ 18
?
Methyl Stearate
Fatty Acid Methyl Ester C ^ 20
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
?
?
?
?
?
7
Approximate
Level (PPB)
8
2
1
2
12
1
4
9
2
18
5
8
8
7
1
2
2
2
-------
10
TABLE B15
Organic Compounds Identified in Sample # 5B
Relative
Retention
Peak # Time
1
2
3
4
5
6
Compounds in Base Extract
Tetrachloroethylene
Diethoxyethane
Camphor (IS)
?
Diethyl-Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
2
4
1
1
1
TABLE B16
Organic Compounds Identified in Sample # 6S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
n
12
13
14
Volatile Compounds
Dichloromethane
Acetone
Tetrahydrofuran
Chloroform
Dioxane
Pentane
Trichloroethylene
Benzene
Hexane
Diisopropyl Ether
Tetrachloroethylene
Toluene
Ethyl benzene
Dichlorobenzene
Approximate
Level (PPB)
2
4
1
1
1
1
6
2
1
1
4
2
1
1
-------
11
TABLE B17
Organic Compounds Identified in Sample # 6A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Peak #
1
2
3
4
5
6
Relative
Retention
Time
0.463
0.791
0.878
0.900
0.933
0.955
1.000
1.060
1.097
1.184
1.218
1.264
1.318
1.342
Organic
Relative
Retention
Time
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C = 12
Fatty Acid Methyl Ester C >_ 13
Fatty Acid Methyl Ester C = 14
Fatty Acid Methyl Ester C >_ 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 20
Fatty Acid Methyl Ester C >_ 21
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
TABLE B18
Compounds Identified in Sample #6B
Compounds in Base Extract
Tetrachl oroethyl ene
Diethoxyethane
Camphor (IS)
?
Diethyl Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
1
1
1
2
1
10
2
8
1
6
1
1
2
Approximate
Level (PPB)
3
5
1
1
4
-------
12
TABLE B19
Organic Compounds Identified in Sample #7S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
Volatile Compounds
?
Dichloromethane
Acetone
Butene
Trichloro-trifluoroethane
Dichloroethylene
Cyclopentane
Tetrahydrofuran
Diethyl Ether
Chloroform
Pentane
Hexene
Trichloroethylene
Benzene
Hexane
Tetrachloroethylene
Toluene
Acetophenone
Chlorobenzene
Nonene
Ethyl benzene
Approximate
Level (PPB)
1
30
2
2
30
2
4
1
5
30
9
5
10
7
10
1
5
2
2
1
4
-------
13
TABLE B20
Organic Compounds Identified in Sample # 7A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
Peak #
Relative
Retention
Time
0.558
0.766
0.851
0.919
0.962
1.000
1.049
1.081
1.143
1.151
1.177
1.210
1.215
1.239
1.270
1.332
1.365
1.386
Organic
Relative
Retention
Time
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C,Q - Terpineol
Methyl -2(4-chlorophenoxy) Butanoate
Methyl Myri state
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 20
?
?
Fatty Acid Methyl Ester C >_ 22
Butyl benzyl Phthalate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
?
?
TABLE B21
Compounds Identified in Sample # 7B
Compounds in Base Extract
Approximate
Level (PPB)
1
1
1
3
5
5
11
1
1
11
2
2
2
2
1
1
1
Approximate
Level (PPB)
1 1.000
2 1.180
Naphthalene (IS)
-------
14
TABLE B22
Organic Compounds Identified in Sample #8S (Field Stripped)
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8 -
9
10
11
Volatile Compounds
Dichloromethane
Acetone
Trichlorofluoromethane
Chloroform
Pentane
Bromo-dichloromethane
Trichloroethylene
Benzene
Hexane
Toluene
Chlorobenzene
Approximate
Level (PPB)
2
2
4
6
6
4
2
2
5
1
1
TABLE B23
Organic Compounds Identified in Sample #8A (Field Extracted)
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1 0.560 Methyl-2-ethyl Hexanoate (IS)
-------
15
TABLE B24
Organic Compounds Identified in Sample #8B (Field Extracted)
Peak #
1
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time Compounds in Base Extract
1.000 Naphthalene (IS)
TABLE B25
Organic Compounds Identified in Sample #8S
Relative
Retention
Time Volatile Compounds
Dichloromethane
Acetone
Butene
Trichloro-fluoromethane
Chloroform
Pentane
?
?
Bromo-dichloromethane
Hexane
Benzene
Dibromo-chloromethane
Methyl Methacrylate
Furfural
Toluene
Chlorobenzene
Approximate
Level (PPB)
(Lab Stripped)
Approximate
Level (PPB)
3
1
1
3
10
1
1
1
7
4
6
3
10
2
1
4
-------
16
TABLE B26
Organic Compounds Identified in Sample # 8A (Lab Extracted)
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1 0.560 Methyl-2-ethyl Hexanoate (IS)
TABLE B27
Organic Compounds Identified in Sample # 8B (Lab Extracted)
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Naphthalene (IS)
-------
17
TABLE B28
Organic Compounds Identified in Sample #9S (Field Stripped)
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Volatile Compounds
Dichloromethane
Acetone
Butene
Tri chl oro-f 1 uoromethane
Dichloroethylene
Pentene Isomer
Tetrahydrofuran
Chloroform
Dichloroethane
Pentene Isomer
Trichloroethane
Pentane
Trichloroethylene
Benzene
Hexane
Methyl -isobutyl Ketone
Tetrachl oroethyl ene
Toluene
Ethyl benzene
Approximate
Level (PPB)
5
4
1
20
1
1
1
20
1
9
1
2
5
2
12
1
1
2
1
-------
18
TABLE B29
Organic Compounds Identified in Sample #9A (Field Extracted)
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.556
0.854
0.911
1.000
1.048
1.081
1.104
1.149
1.176
1.208
1.258
1.277
1.312
Organic
Relative
Retention
Time
0.830
1.000
1.106
1.277
1.523
1.583
1.602
1.852
1.924
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl -2 (4-chlorophenoxy) Butanoate
Methyl Myri state
Methyl Palmitate
?
Methyl Stearate
Hydrocarbon C >_ 20
Hydrocarbon C > 22
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
C,r - Terpineol
TABLE B30
Compounds Identified in Sample #9B (
Compounds in Base Extract
Dichlorobenzene Isomer
Naphthalene (IS)
Alkyl Acid Ester (R + R1 > 8)
C,Q - Terpineol
?
Dibutyl Phthalate
Caffeine
Diethyl Hexyl Phthalate
C - Terpineol
Approximate
Level (PPB)
_
1
2
6
2
10
1
1
11
2
3
6
8
Field Extracted)
Approximate
Level (PPB)
1
1
1
4
4
4
3
3
15
-------
19
TABLE B31
Organic Compounds Identified in Sample # 9S (Lab Stripped)
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Volatile Compounds
Dichloromethane
Acetone
Trichlorofluoromethane
Pentene
Tetrahydrofuran
Diethyl Ether
Chloroform
Pentane
Trichloroethane
Hexene
Trichloroethylene
Benzene
Hexane
Tetrachl oroethyl ene
Toluene
Ethyl Benzene
Approximate
Level (PPB)
8
4
20
1
1
3
20
10
1
2
4
1
10
1
2
2
-------
20
TABLE B32
Organic Compounds Identified in Sample # 9A (Lab Extracted)
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.558
0.850
0.911
1.000
1.035
1.081
1.149
1.176
1.208
1.240
1.250
1.277
1.312
Organic
Relative
Retention
Time
0.830
1.000
1.113
1.522
1.583
1.603
1.855
1.922
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl -2(4-chlorophenoxy) Butanoate
Methyl Myri state
Methyl Palmitate
?
Methyl Stearate
Hydrocarbon C >_ 22
?
Fatty Acid Methyl Ester C 1 22
Butyl benzyl Phthalate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C 1 24
C-c - Terpineol
TABLE B33
Compounds Identified in Sample # 9B
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
Alkyl Acid Ester (R + R1 >_8)
?
Dibutyl Phthalate
Caffeine
Diethyl Hexyl Phthalate
C1K - Terpineol
Approximate
Level (PPB)
_
1
2
13
2
19
1
11
2
4
18
6
9
(Lab Extracted)
Approximate
Level (PPB)
1
1
4
4
4
2
2
-------
21
TABLE B34
Organic Compounds Identified in Sample #10S
Relative
Retention
Peak i Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
Volatile Compounds
Dichloromethane
Acetone
Butene
Trichloro-fl uoromethane
Dichloroethylene
Pentene
Tetrahydrofuran
Diethyl Ether
Chloroform
Trifluoro-trichloroethane
Dichloroethane
Pentane
Trichloroethane
Dioxane
Hexene
Dichloropropane
Trichloroethylene
Benzene
Dibromo-chloromethane
Hexane
Tetrachloroethylene
Toluene
Chlorobenzene
Ethyl benzene
Approximate
Level (PPB)
15
6
1
20
1
1
6
8
20
1
1
10
8
1
2
2
10
2
1
12
4
2
1
1
-------
22
TABLE 835
Organic Compounds Identified in Sample # 10A
Peak #
1
2
3
4
5
6
7
8
9
10
11
Peak #
Relative
Retention
Time
0.545
0.916
1.000
1.040
1.050
1.080
1.150
1.170
1.210
1.260
1.318
Organic
Relative
Retention
Time
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Fatty Acid Methyl Ester C ^16
?
Methyl Stearate
Fatty Acid Methyl Ester C ^18
?
Fatty Acid Methyl Ester C >_ 20
Diethyl Hexyl Phthalate
C,r - Terpineol
TABLE B36
Compounds Identified in Sample #10B
Compounds in Base Extract
Approximate
Level (PPB)
6
104
7
15
180
23
28
8
7
8
Approximate
Level (PPB)
1.000 Naphthalene (IS)
-------
23
TABLE B37
Organic Compounds Identified in Sample
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
Volatile Compounds
Dichloromethane
Acetone
Tetrahydrofuran
Diethyl Ether
Chloroform
Dichloroethane
Trichloroethane
Bromo-dichloromethane
Dichloropropane
Trichloroethylene
Benzene
Tetrachl oroethyl ene
Approximate
Level (PPB)
8
1
1
1
5
1
4
1
1
5
1
4
-------
24
TABLE B38
Organic Compounds Identified in Sample #11A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
Peak #
1
2
Relative
Retention
Time
0.590
0.833
0.840
0.850
0.919
0.960
1.000
1.030
1.045
1.077
1.113
1.146
1.170
1.208
1.253
1.274
1.289
1.307
Organic
Relative
Retention
Time
1.000
1.862
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C = 12
Methyl Trichlorophenyl Ether
Methyl -2-(4-chlorophenoxy) Butanoate
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
+ Methyl Pentachlorophenoxy Ether
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 18
Methyl Arachidate
?
Fatty Acid Methyl Ester C >_ 20
Diethyl Hexyl Phthalate
?
?
C-.C Terpineol
TABLE B39
Compounds Identified in Sample # 11B
Compounds in Base Extract
Naphthalene (IS)
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
22
14
11
24
24 (mix)
94
12
26
131
10
27
49
32
23
25
17
21
Approximate
Level (PPB)
_
1
-------
25
TABLE B40
Organic Compounds Identified in Sample #12S (Nonchlorinated)
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Volatile Compounds
Dichloromethane
Acetone
Butene
Tri chl oro-f 1 uoromethane
Dichloroethylene
Tetrahydrofuran
Diethyl Ether
Chloroform
Pentane
Trichloroethane
Dioxane
Tetrahydropyran
Tri chl oroethy 1 ene
Benzene
CrHgO or C,H,,,0
Methyl -tetrahydropyran
Cu fi r\v* c u n
c 1 n c i o
Tetrachloroethylene
Toluene
Acetophenone
Approximate
Level (PPB)
3
1
3
5
1
3
10
20
6
4
1
9
4
1
10
2
4
5
1
1
-------
26
TABLE B41
Organic Compounds Identified in Sample #12S (Chlorinated)
Relative
Retention
Peak i Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
Volatile Compounds
Dichloromethane
Acetone
Butene
Trichloro-fluoromethane
Dichloroethylene
Tetrahydrofuran
Di ethyl Ether
Chloroform
?
Pentane
Trichloroethane
Dioxane
Tetrahydropyran
Trichloroethylene
Benzene
Dimethyl formamide
CgHgO or CgH,20
Methyl -tetrahydropyran
C5H1Q0 or C6H]20
N ,N-Dimethyl acetamide
Tetrachloroethylene
Dichlorobenzene Isomer
Dichlorobenzene Isomer
Approximate
Level (PPB)
3
2
5
4
1
4
10
14
1
2
6
2
9
4
2
2
14
4
6
2
4
2
2
-------
27
TABLE B42
Organic Compounds Identified in Sample # 12A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
Relative
Retention
Time
0.572
0.670
0.717
0.753
0.768
0.830
0.854
0.917
0.943
0.964
1.000
1.040
1.047
1.077
1.112
1.137
1.148
1.175
1.208
1.261
i:277
1.294
1.312
1.324
1.335
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
Methyl Dichlorophenyl Ether
?
Methyl Trichlorophenyl Ether
C,n - Terpineol
Fatty Acid Methyl Ester C = 12
Methyl -2- (4-chlorophenoxy) Butanoate
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Methyl Stearate
?
?
Methyl Arachidate
?
Fatty Acid Methyl Ester C >_ 22
+ Methyl Dehydroabietate
Diethyl Hexyl Phthalate
7
7
7
7
7
5
8
10
15
4
4
18
31
26
117
19
27
173
24
23
25
60
90 (mix)
137
50
68
50
52
68
-------
28
TABLE 843
Organic Compounds Identified in Sample # 12B
Peak if
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.810
1.000
1.103
1.620
1.699
1.754
1.830
1.873
1.952
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
Alkyl Acid Ester (R + R1 >_ 8)
Caffeine
?
?
?
Diethyl Hexyl Phthalate
C,5 - Terpineol
Approximate
Level (PPB)
16
2
1
9
4
2
1
1
TABLE B44
Organic Compounds Identified in Sample # 13S
Peak #
1
2
3
4
5
Relative
Retention
Time
_
Volatile Compounds
Chloroform
Bromo-dichloromethane
Trichloroethylene
Benzene
Chi oro benzene
Approximate
Level (PPB)
8
4
2
3
1
-------
29
TABLE B45
Organic Compounds Identified in Sample #13A
Peak #
1
2
3
4
Relative
Retention
Time
0.545
1.000
1.263
1.320
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
Diethyl Hexyl Phthalate
C,j. - Terpineol
Approximate
Level (PPB)
_ _ _
1
1
1
TABLE B46
Organic Compounds Identified in Sample #13B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Naphthalene (IS)
-------
30
TABLE B47
Organic Compounds Identified in Sample # 14S
Peak #
1
2
3
4
5
6
7
8
9
10
11
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time
_
Organic
Relative
Retention
Time
0.557
0.853
0.902
0.919
0.940
1.000
1.078
1.138
1.260
1.293
1.423
1.447
Volatile Compounds
Trichloro-fluoromethane
Neopentane
Chloroform
Trichloroethane
Hexene Isomer
Hexene Isomer
1-Bromo-l-chloroethane
Benzene
Dibromoethane
Methyl -isobutyl Ketone
Heptene
TABLE B48
Compounds Identified in Sample # 14A
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Hydrocarbon C > 16
Hydrocarbon C > 18
Fatty Acid Methyl Ester C ^ 14
Hydrocarbon C > 18
Methyl Palmitate
Methyl Stearate
ci6Hio (pyrene?)
Diethyl Hexyl Phthalate
(C,gH12) Benzanthrene
?
?
Approximate
Level (PPB)
1
2
1
2
1
1
1
1
10
2
1
Approximate
Level (PPB)
2
2
2
1
2
5
1
1
1
8
8
-------
31
TABLE B49
Organic Compounds Identified in Sample #148
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.474
1.000
1.235
1.270
1.346
1.625
1.657
1.708
1.741
1.856
1.887
1.944
1.968
Compounds in Base Extract
Dibromoethane
Naphthalene (IS)
Hydrocarbon C >_ 16
Hydrocarbon C >_ 16
Hydrocarbon C ^ 18
Caffeine
Hydrocarbon C >_ 22
Hydrocarbon C >_ 22
ci6Hio (pyrene)
Benzylbutyl Phthalate
Di ethyl Hexyl Phthalate
Hydrocarbon C >_ 28
Terpineol
Approximate
Level (PPB)
6
1
1
1
2
1
1
1
1
4
1
4
-------
32
TABLE B50
Organic Compounds Identified in Sample # IBS
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
Peak #
1
2
3
4
5
Relative
Retention
Time
Organic
Relative
Retention
Time
0.575
1.000
1.060
1.250
1.300
Volatile Compounds
Dichloromethane
Acetone
Trichloro-fl uoromethane
Dichloroethylene
Chloroform
Pentane
Dichloroethane
Trichloroethane
Hexene
Trichloroethylene
Benzene
Tetrachloroethylene
Chlorobenzene
TABLE B51
Compounds Identified in Sample # ISA
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Pa Imitate
Methyl Stearate
Diethyl Hexyl Phthalate
C,r - Terpineol
Approximate
Level (PPB)
1
1
1
2
1
1
6
1
4
6
2
3
1
Approximate
Level (PPB)
1
1
5
4
-------
33
TABLE B52
Organic Compounds Identified in Sample # 15B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Naphthalene (IS)
TABLE B53
Organic Compounds Identified in Sample #16S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Volatile Compounds
Dichloromethane
Acetone
Butene
Trichloro-fluoromethane
Dichloroethylene
Diethyl Ether
Chloroform
Pentane
Tetrahydropyran
Trichloroethylene
Benzene
Hexane
Tetrachl oroethyl ene
Toluene
Chlorobenzene
Approximate
Level (PPB)
2
1
1
12
2
5
20
8
3
5
4
10
4
2
1
-------
34
TABLE B54
Organic Compounds Identified in Sample # 16A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.579
0.770
0.850
0.900
0.920
0.960
1.000
1.040
1.044
1.070
1.140
1.170
1.210
1.250
1.257
1.270
1.280
1.300
1.320
1.330
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
C,n - Terpineol
Hydrocarbon C > 18
+ Methyl -2(4-chlorophenoxy) Butanoate
Fatty Acid Methyl Ester C >. 14
Fatty Acid Methyl Ester C >_ 14
Fatty Acid Methyl Ester C > 14
+ Methyl Pentachlorophenyl Ether
Methyl Palmitate
Fatty Acid Methyl Ester C i 16
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 18
?
Fatty Acid Methyl Ester C >_ 20
Di ethyl Hexyl Phthalate
?
?
?
?
?
?
10
10 (mix)
21
20
25 (mix)
70
9
29
79
34
85
33
50
25
35
25
30
43
41
-------
35
TABLE B55
Organic Compounds Identified in Sample # 16B
Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.811
1.000
1.102
1.429
1.594
1.618
1.873
1.952
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
C,0 - Terpineol
Dimethyl Biphenyl
Di butyl Phthalate
Caffeine
Di ethyl Hexyl Phthalate
C - Terpineol
15
Approximate
Level (PPB)
18
1
1
1
1
1
1
TABLE B56
Organic Compounds Identified in Sample ti 17S
Peak #
1
2
Relative
Retention
Time
0.548
1.000
Volatile Compounds
Dichloromethane
Chloroform
Approximate
Level (PPB)
1
2
-------
36
TABLE 857
Organic Compounds Identified in Sample #17A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time
0.563
0.739
0.763
0.846
0.913
1.959
1.000
1.062
1.075
1.113
1.175
1.207
1.213
1.261
1.277
1.312
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Trichlorophenyl Ether
C,Q - Terpineol
Methyl -2 (4-chlorophenoxy) Butanoate
Fatty Acid Methyl Ester C = 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
?
Methyl Dehydroabietate
Butyl phthalyl butyl Glycolate
Di ethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
C,r - Terpineol
Approximate
Level (PPB)
12
10
10
7
43
81
10
45
55
45
37
48
85
52
104
-------
37
TABLE B58
Organic Compounds Identified in Sample # 17B
Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.812
1.000
1.112
1.463
1.623
1.843
1.887
1.963
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
C.Q - Terpineol
?
Caffeine
?
Di ethyl Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
4
1
1
2
1
1
1
TABLE B59
Organic Compounds Identified in Sample # 18S
Peak 1
1
2
3
4
Relative
Retention
Time
1.000
1.307
1.569
2.126
Volatile Compounds
Chloroform
Bromo-dichloromethane
Dibromo-chloromethane
Toluene
Approximate
Level (PPB)
13
2
4
1
-------
38
TABLE B60
Organic Compounds Identified in Sample # ISA
Peak #
1
. 2
3
4
Relative
Retention
Time
0.453
0.828
1.000
1.098
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C,n - Terpineol
Methyl Palmitate
Methyl Stearate
Approximate
Level (PPB)
1
1
1
TABLE B61
Organic Compounds Identified in Sample # 18B
Peak #
1
2
3
4
Relative
Retention
Time
1.000
1.492
1.968
2.385
Compounds in Base Extract
Camphor (IS)
C-.Q - Terpineol
Dibutyl Phthalate
Diethyl Phthalate
Approximate
Level (PPB)
3
1
4
-------
39
TABLE B62
Organic Compounds Identified in Sample # 19S
Relative ....
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
Sample #19 was not assayed for volatiles.
-------
40
TABLE B63
Organic Compounds Identified in Sample #19A
Peak §
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Relative
Retention
Time
0.550
0.817
0.890
0.948
1.000
1.024
1.064
1.106
1.131
1.143
1.188
1.213
1.234
1.277
1.286
1.316
1.347
1.372
1.396
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C10 - Terpineol
Methyl Myri state
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
?
Methyl Stearate
?
Hydrocarbon C >_ 22
Hydrocarbon C > 24
?
?
Methyl Dehydroabietate
Fatty Acid Methyl Ester C >_ 22
Hydrocarbon C > 26
Di ethyl Hexyl Phthalate
?
Hydrocarbon C > 30
Approximate
Level (PPB)
7
5
10
61
8
5
56
17
18
20
19
52
15
35
22
38
27
20
-------
41
TABLE B64
Organic Compounds Identified in Sample #19B
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.511
2.011
2.175
2.258
2.351
2.461
Compounds in Base Extract
Camphor (IS)
C,Q - Terpineol
Dibutyl Phthalate
Hydrocarbon C > 22
Hydrocarbon C > 24
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
2
4
1
1
3
1
TABLE B65
Organic Compounds Identified in Sample # 20S
Peak #
1
2
3
Relative
Retention
Time
1.000
1.533
2.221
Volatile Compounds
Chloroform
Benzene
Chlorobenzene
Approximate
Level (PPB)
12
2
1
-------
42
TABLE B66
Organic Compounds Identified in Sample # 20A
Peak #
1
2
3
Relative
Retention
Time
0.455
1.100
1.093
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level (PPB)
1
1
TABLE B67
Organic Compounds Identified in Sample #20B
Peak #
Relative
Retention
Time
Compounds in Base Extract
Approximate
Level (PPB)
1.000
Camphor (IS)
-------
43
TABLE B68
Organic Compounds Identified in Sample # 21S
Peak i
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.862
1.000
1.085
1.195
1.303
1.515
1.543
1.978
2.036
2.127
Volatile Compounds
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Tetrahydropyran
Trichloroethylene
Benzene
Dichlorobenzene
Tetrachloroethylene
Toluene
Approximate
Level (PPB)
1
16
1
3
2
1
1
1
2
1
-------
44
TABLE B69
Organic Compounds Identified in Sample # 21A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Relative
Retention
Time
0.499
0.666
0.899
1.000
1.048
1.058
1.091
1.131
1.170
1.179
1.200
1.215
1.254
1.261
1.315
1.346
1.361
1.379
1.400
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Hydrocarbon C >_ 14
Methyl Myri state
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Methyl Stearate
?
C16H10 lsomer
Fatty Acid Methyl Ester C >_ 20
C,nH,n Isomer
?
Methyl Dehydroabietate
Fatty Acid Methyl Ester
Diethyl Hexyl Phthalate
?
?
?
?
Approximate
Level (PPB)
1
2
22
3
3
33
2
1
10
1
12
4
5
20
8
6
5
2
-------
45
TABLE B70
Organic Compounds Identified in Sample #21B
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.405
2.384
2.455
2.701
2.739
2.799
Compounds in Base Extract
Camphor (IS)
Hydrocarbon C > 16
Di ethyl Hexyl Phthalate
C18H12
?
?
?
Approximate
Level (PPB)
- _ _
1
7
1
1
8
6
TABLE B71
Organic Compounds Identified in Sample #22S
Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.485
0.867
1.000
1.072
1.172
1.393
1.481
1.985
Volatile Compounds
Acetone
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
1 ,2-Dichloropropane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level (PPB)
2
1
22
1
1
2
7
1
-------
46
TABLE B72
Organic Compounds Identified in Sample # 22A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.438
0.787
0.797
0.815
0.827
0.897
0.951
1.000
1.018
1.057
1.097
1.185
1.218
1.263
1.318
1.324
1.339
1.364
1.385
1.400
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C >_ 12
Methyl Trichlorophenyl Ether
Methyl -2(4-chlorophenoxy) Butanoate
Methyl Tetrachlorophenyl Ether
Methyl Myri state
Methyl Pentachlorophenyl Ether
Methyl Palmitate
Alkyl Benzene
?
Methyl Stearate
Fatty Acid Methyl Ester C ^ 20
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
7
?
?
C,5 ~ Terpineol
?
1
1
1
2
1
1
2
1
2
3
1
8
4
2
2
2
1
1
1
-------
47
TABLE B73
Organic Compounds Identified in Sample # 22B
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
Peak i
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.313
1.526
1.609
1.755
1.800
1.889
2.007
2.097
2.147
2.208
2.302
2.432
Organic
Relative
Retention
Time
0.427
0.861
0.959
1.000
1.087
1.197
1.434
1.527
2.054
Compounds in Base Extract
Camphor (IS)
Hydrocarbon
?
?
Diphenyl Ethane
Alkyl Phenyl Ether
?
Dibutyl Phthalate
?
C16H10
C16H10
?
Diethyl Hexyl Phthalate
TABLE B74
Compounds Identified in Sample ft 23S
Volatile Compounds
Dichloromethane
Tetrahydrofuran
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
1 ,2-Dichloropropane
Trichloroethylene
Tetrachloroethylene
Approximate
Level (PPB)
1
3
3
3
4
2
1
1
1
3
2
5
Approximate
Level (PPB)
1
2
1
27
2
1
1
5
1
-------
48
TABLE B75
Organic Compounds Identified in Sample #23A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time
0.446
0.814
0.897
0.951
0.969
1.000
1.057
1.097
1.215
1.264
1.326
1.347
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
Methyl -2(4-chlorophenoxy) Butanoate
Fatty Acid Methyl Ester C = 14
Fatty Acid Methyl Ester C >_ 14
Alkyl Benzene
Methyl Palmitate
?
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 22
Di ethyl Hexyl Phthalate
?
2
2
2
3
2
2
3
6
3
1
2
TABLE B76
Organic Compounds Identified in Sample #23B
Peak #
1
2
3
4
Relative
Retention
Time
1.000
1.963
2.275
2.374
Compounds in Base Extract
Camphor (IS)
Di butyl Phthalate
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
_ _ _
2
6
2
-------
49
TABLE B77
Organic Compounds Identified in Sample # 24S
Peak #
1
2
3
4
5
6
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Relative
Retention
Time
0.954
1.000
1.075
1.184
1.512
2.036
Organic
Relative
Retention
Time
0.436
0.812
0.933
0.952
1.000
1.057
1.094
1.215
1.254
1.269
1.318
1.342
1.363
1.384
1.403
1.436
1.463
Volatile Compounds
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
TABLE B78
Compounds Identified in Sample # 24A
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl -2(4-chlorophenoxy) Butanoate
Hydrocarbon C >_ 16
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
?
?
Di ethyl Hexyl Phthalate
?
Hydrocarbon C >_ 28
C,,- - Terpineol
1 D
Hydrocarbon C ^ 30
Hydrocarbon C >_ 30
Hydrocarbon C >_ 30
Approximate
Level (PPB)
1
17
1
1
2
2
Approximate
Level (PPB)
2
1
1
2
2
3
9
3
1
1
3
1
1
1
1
1
-------
50
TABLE B79
Organic Compounds Identified in Sample # 24B
Peak #
1
2
3
4
5
Relative
Retention
Time
1.000
1.991
2.356
2.411
2.522
Compounds in Base Extract
Camphor (IS)
Dibutyl Phthalate
Butyl benzyl Phthalate
Diethyl Hexyl Phthalate
C,r - Terpineol
Approximate
Level (PPB)
2
1
1
1
TABLE B80
Organic Compounds Indentified in Sample # 25S
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
0.864
0.954
1.000
1.079
1.187
1.493
1.998.
Volatile Compounds
Tetrahydrofuran
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level (PPB)
2
1
26
1
1
1
1
-------
51
TABLE B81
Organic Compounds Identified in Sample # 25A
Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.448
1.000
1.058
1.094
1.206
1.254
1.321
1.346
1.385
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
?
Diethyl Hexyl Phthalate
?
C,r - Terpineol
Approximate
Level (PPB)
2
2
3
6
2
1
2
2
TABLE B82
Organic Compounds Identified in Sample #25B
Peak #
1
2
3
Relative
Retention
Time
1.000
2.013
2.441
Compounds in Base Extract
Camphor (IS)
Dibutyl Phthalate
Diethyl hexyl Phthalate
Approximate
Level (PPB)
_ _
1
1
-------
52
TABLE B83
Organic Compounds Identified in Sample # 26S
Peak #
1
2
3
4
5
6
7
Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.396
0.957
1.000
1.141
1.483
1.509
1.983
Organic
Relative
Retention
Time
0.468
0.951
1.000
1.057
1.094
1.215
1.322
1.347
1.386
Volatile Compounds
Dichloromethane
Dichloroethylene
Chloroform
1 ,1 ,1-Trichloroethane
Trichloroethylene
Benzene
Tetrachl oroethyl ene
TABLE B84
Compounds Identified in Sample # 26A
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
?
C,c - Terpineol
Approximate
Level (PPB)
1
1
20
1
1
1
1
Approximate
Level (PPB)
1
2
1
3
4
2
2
2
-------
53
TABLE B85
Organic Compounds Identified in Sample #26B
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.985
2.413
2.441
2.530
2.647
2.780
Compounds in Base Extract
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
?
C,r - Terpineol
?
?
Approximate
Level (PPB)
1
2
1
4
2
2
TABLE B86
Organic Compounds Identified in Sample # 27S
Relative
Retention Approximate
Peak i Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 14
-------
54
TABLE B87
Organic Compounds Identified in Sample #27A
Peak #
1
2
3
4
5
6
Relative
Retention
Time
0.468
0.960
1.000
1.097
1.222
1.319
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C Cl F n * 4
n x z -
Methyl Palmitate
Methyl Stearate + C Cl F , n % 4
II n £
C Cl F n ^ 4
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
2
1
4 (mix)
2
1
TABLE B88
Organic Compounds Identified in Sample # 27B
Peak #
1
2
3
4
Relative
Retention
Time
1.000
1.977
2.397
2.513
Compounds in Base Extract
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C1(; - Terpineol
Approximate
Level (PPB)
2
1
1
-------
55
TABLE B89
Organic Compounds Identified in Sample # 28S
Peak #
1
2
3
4
5
6
Peak #
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
1.000
1.189
1.516
1.544
2.031
2.123
Organic
Relative
Retention
Time
0.464
0.907
0.945
1 . 000
1:058
1.095
1.221
1.329
1.357
1.375
1.397
Volatile Compounds
Chloroform
1 ,1 ,1-Trichloroethane
Trichloroethylene
Benzene
Tetrachloroethylene
Toluene
TABLE B90
Compounds Identified in Sample # 28A
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
7
Methyl Pentachlorophenyl Ether
Methyl Palmitate
7
Methyl Stearate
7
Diethyl Hexyl Phthalate
7
7
C1C - Terpineol
Approximate
Level (PPB)
18
1
1
1
1
1
Approximate
Level (PPB)
2
1
2
2
3
4
2
2
1
1
-------
56
TABLE B91
Organic Compounds Identified in Sample #28B
Peak #
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.499
1.991
2.326
2.432
2.466
Compounds in Base Extract
Camphor (IS)
CIQ - Terpineol
Dibutyl Phthalate
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
?
Approximate
Level (PPB)
...
1
1
2
3
3
TABLE B92
Organic Compounds Identified in Sample # 29S
Relative
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 14
2 1.504 Trichloroethylene 1
3 1.532 Benzene 1
-------
57
TABLE B93
Organic Compounds Identified in Sample # 29A
Peak #
1
2
3
4
5
6
7
Peak #
1
2
3
4
5
Relative
Retention
Time
0.451
1.000
1.056
1.096
1.223
1.325
1.394
Organic
Relative
Retention
Time
1.000
1.962
2.386
2.413
2.502
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
C,r - Terpineol
TABLE B94
Compounds Identified in Sample #29B
Compounds in Base Extract
Camphor (IS)
Di butyl Phthalate
Diethyl Hexyl Phthalate
?
Terpineol
Approximate
Level (PPB)
2
1
2
3
1
1
Approximate
Level (PPB)
...
1
1
1
2
-------
58
TABLE B95
Organic Compounds Identified in Sample #30S
Peak #
1
2
3
4
5
Relative
Retention
Time
1.000
1.262
1.507
1.535
2.230
Volatile Compounds
Chloroform
?
Trichloroethylene
Benzene
Acetophenone
Approximate
Level (PPB)
120
10
1
1
1
TABLE B96
Organic Compounds Identified in Sample #30A
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
0.442
1.000
1.058
1.094
1.215
1.321 .
1.385
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
C c - Terpineol
Approximate
Level (PPB)
1 ,
1
2
3
1
1
-------
59
TABLE B97
Organic Compounds Identified in Sample #30B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Camphor (IS)
2 1.995 Dibutyl Phthalate 1
3 2.422 Diethyl hexyl Phthalate 1
4 2.457 ? 1
TABLE B98
Organic Compounds Identified in Sample #31S
Relative
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 14
2 1.535 Trichloroethylene 1
3 1.564 Benzene 1
4 1.995 Tetrachloroethylene 1
-------
60
TABLE B99
Organic Compounds Identified in Sample i 31A
Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.442
0.551
0.567
0.607
1.000
1.092
1.215
1.261
1.316
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
?
?
?
Methyl Palmitate
Methyl Stearate
?
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
1
1
1
3
3
2
4
1
TABLE B100
Organic Compounds Identified in Sample # 31B
Peak #
1
2
3
Relative
Retention
Time
1.000
2.409
2.527
Compounds in Base Extract
Camphor (IS)
Diethyl Hexyl Phthalate
C,r - Terpineol
Approximate
Level (PPB)
___
1
2
-------
61
TABLE B101
Volatile Organic Compounds Identified in Sample No. 32S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.729
1.000
1.006
1.583
2.295
Compound
Dimethoxymethane
Chloroform
1 ,2-Dichloroethane
Benzene
Chlorobenzene
Approximate
Level
(ppb)
2
2
2
1
1
TABLE B102
Organic Compounds Identified in Acid Extract of Sample No. 32A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.464
1.000
1.094
1.265
1.322
1.386
1.450
1.526
Compound
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C-, 5 Terpineol
?
?
Approximate
Level
(ppb)
...
3
3
2
2
1
1
1
-------
62
TABLE B103
Organic Compounds Identified in Base Extract of Sample No.32B
Peak
No.
1
2
3
4
5
6
7
8
9
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.107
1.207
1.237
1.521
2.043
2.398
2.511
2.648
Volatile
Relative
Retention
Time
0.735
0.868
1.000
1.081
1.524
2.047
Compound
Camphor (IS)
?
Nitrotoluene
Chloro-Nitrobenzene
C,Q - Terpineol
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C,5 - Terpineol
TABLE B104
Organic Compounds Identified in Sample No.
Compound
Dimethoxymethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
___
4
4
17
1
1
1
49
1
33S
Approximate
Level
(ppb)
1
1
2
1
1
1
-------
63
TABLE B105
Organic Compounds Identified in Acid Extract of Sample No.33A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.483
0.502
0.955
1.000
1.020
1.103
1.350
1.372
1.420
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
?
Methyl Palmitate
?
Methyl Stearate
Di ethyl Hexyl Phthalate
Fatty Acid Methyl Ester C > 22
C,r - Terpineol
Approximate
Level
(ppb)
_ _ _
1
25
4
1
3
1
1
2
-------
64
TABLE B106
Organic Compounds Identified in Base Extract of Sample No. 33B
Peak
No.
1
2
3
4
5
6
7
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.827
1.000
1.101
1.208
1.244
1.657
2.514
Volatile
Relative
Retention
Time
0.719
0.862
1.000
1.086
1.532
2.053
Compound
Dichlorobenzene
Camphor (IS)
?
Nitrotoluene
Chloronitrobenzene
Dinitrotoluene
Diethyl Hexyl Phthalate
TABLE B107
Organic Compounds Identified in Sample No.
Compound
Dimethoxymethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
TABLE BIOS
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
Relative
Retention
Time
0.500
1.000
1.084
1.289
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
3
1
1
2
1
1
34S
Approximate
Level
(ppb)
3
1
2
12
2
3
N0.34A
Approximate
Level
(ppb)
2
2
1
-------
65
TABLE B109
Organic Compounds Identified in Base Extract of Sample No. 34B
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
2.037
2.499
2.630
Compound
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
C,c Terpineol
Approximate
Level
(ppb)
-. _ _
1
2
3
TABLE B110
Volatile Organic Compounds Identified in Sample No. 35S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.749 Dimethoxymethane 3
2 1.000 Chloroform 2
3 1.082 1,2-Dichloroethane 15
4 1.507 Trichloroethylene 1
5 2.004 Tetrachloroethylene 3
-------
66
TABLE Bill
Organic Compounds Identified in Acid Extract of Sample No.35A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.490
1.000
1.102
1.349
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_
2
2
1
TABLE B112
Organic Compounds Identified in Base Extract of Sample No. 35B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B113
Volatile Organic Compounds Identified in Sample No. 36S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.710
1.000
1.069
1.535
2.063
Compound
Dimethoxymethane
Chloroform
1,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
3
7
9
1
2
-------
67
TABLE B114
Organic Compounds Identified in Acid Extract of Sample No. 36A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0/450
0.958
1.000
1.099
1.336
1.401
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C-.C - Terpineol
Approximate
Level
(ppb)
-
19
6
11
1
1
TABLE B115
Organic Compounds Identified in Base Extract of Sample No. 36B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.380 Diethyl Hexyl Phthalate 1
-------
68
TABLE B116
Volatile Organic Compounds Identified in Sample No. 37S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.730
1.000
1.079
1.461
1.917
Compound
Dimethoxymethane
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
4
2
15
1
2
TABLE B117
Organic Compounds Identified in Acid Extract of Sample No. 37A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.453 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.098 Methyl Stearate 5
-------
69
TABLE B118
Organic Compounds Identified in Base Extract of Sample No. 37B
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.897
2.431
Compound
Camphor (IS)
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
1
TABLE B119
Volatile Organic Compounds Identified in Sample No. 38S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.414 Dichloromethane 2
2 0.489 Acetone 2
3 0.722 Dimethoxymethane 2
4 1.000 Chloroform 2
5 1.087 1,2-Dichlorqethane 11
6 1.447 1,2-Dichloropropane 1
7 1.537 Trichloroethylene 1
8 1.568 Benzene 1
9 2.050 Tetrachloroethylene 1
-------
70
TABLE B120
Organic Compounds Identified in Acid Extract of Sample No. 38A
Peak
No.
1
2
3
Relative
Retention
Time
0.450
1.000
1.096
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
_
3
3
TABLE B121
Organic Compounds Identified in Base Extract of Sample No.38B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.627 ? 2
-------
71
TABLE B122
Volatile Organic Compounds Identified in Sample No. 39S
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.491
0.759
1.000
1.077
1.175
1.394
1.509
1.973
2.061
Compound
Dichloromethane
Methyl al
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
1 ,2-Dichloropropane
Trichloroethylene
Tetrachl oroethyl ene
Toluene
Approximate
Level
(Ppb)
8
12
12
90
1
2
24
4
1
TABLE B123
Organic Compounds Identified in Acid Extract of Sample No. 39A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.452
1.000
1.095
1.327
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
6
8
1
-------
72
TABLE B124
Organic Compounds Identified in Base Extract of Sample No.39B
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.572
1.627
1.991
2.249
2.431
2.508
2.684
2.833
Compound
Camphor (IS)
?
?
Dibutyl Phthalate
?
Diethyl Hexyl Phthalate
Unidentified Phthalate
?
?
Approximate
Level
(ppb)
_
1
3
1
1
1
1
1
1
TABLE B125
Volatile Organic Compounds Identified in Sample No. 40S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.524 Trichloroethylene 2
3 2.036 Tetrachloroethylene 1
-------
73
TABLE B126
Organic Compounds Identified in Acid Extract of Sample No. 40A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.467
1.000
1.099
1.329
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
2
3
1
TABLE B127
Organic Compounds Identified in Base Extract of Sample No. 40B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.612 ? 2
3 2.416 Diethyl Hexyl Phthalate 2
4 2.662 ? 4
5 2.790 ? 2
-------
74
TABLE B128
Volatile Organic Compounds Identified in Sample No. 41S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 6
2 1.500 Trichloroethylene 1
3 2.054 Tetrachloroethylene 1
TABLE B129
Organic Compounds Identified in Acid Extract of Sample No. 41A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.472
1.000
1.093
1.326
1.458
1.517
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
?
?
Approximate
Level
(ppb)
6
6
2
4
3
-------
75
TABLE B130
Organic Compounds Identified in Base Extract of Sample No. 41B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.612 ? 1
3 2.420 Diethyl Hexyl Phthalate 1
4 2.662 ? 2
TABLE B131
Volatile Organic Compounds Identified in Sample No. 42S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 13
2 1.086 1,2-Dichloroethane 8
3 1.507 Trichloroethylene 4
4 2.053 Tetrachloroethylene 5
-------
76
TABLE B132
Organic Compounds Identified in Acid Extract of Sample No. 42A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.450
1.000
1.096
1.331
1.397
1.466
1.546
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C,5 - Terpineol
?
?
Approximate
Level
(PPb)
___
5
6
1
1
2
2
TABLE B133
Organic Compounds Identified in Base Extract of Sample No. 42B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.850 Dichlorobenzene 3
2 1.000 Camphor (IS)
3 1.102 Nitrotoluene 7
4 1.236 Chloronitrobenzene 13
5 2.381 Diethyl Hexyl Phthalate 1
6 2.622 ? 3
7 2.772 ? 3
-------
77
TABLE B134
Volatile Organic Compounds Identified in Sample No. 43S
Peak
No.
1
2
3
Relative
Retention
Time
0.535
1.000
1.505
Compound
Acetone
Chloroform
Trichloroethylene
Approximate
Level
(ppb)
1
2
2
TABLE B135
Organic Compounds Identified in Acid Extract of Sample No. 43A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.450
1.000
1.097
1.200
1.240
1.333
1.352
1.379
1.400
1.467
1.549
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
?
Dioctyl Adipate
Di ethyl Hexyl Phthalate
Diethyl Hexyl Phthalate
Di ethyl Hexyl Phthalate
C, 5 - Terpineol
?
?
Approximate
Level
(ppb)
4
3
1
11
1
1
1
1
1
1
-------
78
TABLE B136
Organic Compounds Identified in Base Extract of Sample No. 43B
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
2.387
2.546
2.665
2.801
Compound
Camphor (IS)
Di ethyl Hexyl Phthalate
C-.C Terpineol
?
?
Approximate
Level
(ppb)
2
1
2
3
TABLE B137
Volatile Organic Compounds Identified in Sample No. 44S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.736 Dimethoxymethane 2
2 1.000 Chloroform 2
3 2.143 Dichlorobenzene 8
4 2.220 Dichlorobenzene 10
-------
79
TABLE B138
Organic Compounds Identified in Acid Extract of Sample No. 44A
Peak
No.
1
2
3
4
5
7
8
9
10
11
12
13
Relative
Retention
Time
0.456
0.496
0.582
0.638
0.692
0.861
0.896
1.000
1.100
1.207
1.279
1.339
Approximate
Level
Compound (ppb)
Methyl -2-Ethyl Hexanoate (IS)
Methyl -2 ,2-Dichloro-3-Methyl Butanoate
Dichlorinated Hydrocarbon C > 5
Dichlorinated Hydrocarbon C > 5
?
Al kyl Benzene
Methyl Myri state
Methyl Palmitate
Methyl Stearate
C-,r Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
_ _ _
59
21
5
1
1
2
5
4
2
1
1
TABLE B139
Organic Compounds Identified in Base Extract of Sample No.44B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.008 Dibutyl Phthalate 1
3 2.463 Diethyl Hexyl Phthalate 2
4 2.590 C,c Terpineol 1
-------
80
TABLE B140
Volatile Organic Compounds Identified in Sample No. 45S
Peak
No.
1
2
3
Relative
Retention
Time
0.532
1 . 000
1.559
Compound
Acetone
Chloroform
Benzene
Approximate
Level
(ppb)
1
4
1
TABLE B141
Organic Compounds Identified in Acid Extract of Sample No. 45A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.450
0.900
0.959
1.000
1.099
1.200
1.337
1.406
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Hexachloro-hexafluoropentane
Methyl Palmitate
Methyl Stearate.
C, c Terpene
Di ethyl Hexyl Phthalate
C,r - Terpineol
Approximate
Level
(ppb)
___
2
1
6
4
2
1
1
-------
81
TABLE B142
Organic Compounds Identified in Base Extract of Sample No. 45B
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.991
2.384
2.566
2.691
Compound
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
C-,r Terpineol
?
Approximate
Level
(ppb)
1
2
1
1
TABLE B143
Volatile Organic Compounds Identified in Sample No. 46S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.552 Acetone 1
2 1.000 Chloroform 2
3 1.534 Benzene 1
4 2.095 Dichlorobenzene 10
-------
82
TABLE B144
Organic Compounds Identified in Acid Extract of Sample No. 46A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.450
1.000
1.099
1.199
1.282
1.331
1.392
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,r Terpene
Wz
Diethyl Hexyl Phthalate
C, 5 - Terpineol
Approximate
Level
(ppb)
___
5
4
2
1
1
1
TABLE B145
Organic Compounds Identified in Base Extract of Sample No. 46B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.427 Diethyl Hexyl Phthalate 1
3 2.551 C15 Terpineol 1
4 2.675 ? 1
5 2.831 ? 1
-------
83
TABLE B146
Volatile Organic Compounds Identified in Sample No. 47S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B147
Organic Compounds Identified in Acid Extract of Sample No. 47A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.450
1.000
1.095
1.328
1.393
1.463
1.552
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C-,,- - Terpineol
?
?
Approximate
Level
(ppb)
_ _ _
3
2
1
1
1
1
-------
84
TABLE 6148
Organic Compounds Identified in Base Extract of Sample No.47B
Peak
No.
1
2
3
4
5
Peak
No.
Relative
Retention
Time
1.000
2.399
2.516
2.643
2.797
Volatile
Relative
Retention
Time
Compound
Camphor (IS)
Diethyl Hexyl Phthalate
C,5 Terpineol
?
?
TABLE B149
Organic Compounds Identified in Sample No.
Compound
Approximate
Level
(ppb)
_
1
1
2
2
48S
Approximate
Level
(ppb)
No peaks over 1 PPB.
TABLE B150
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.443
1.000
1.096
1.198
1.270
1.397
Compound
Methyl -2-Ethyl Hexanoate (IS)
. Methyl Pa Imitate
Methyl Stearate
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
C, c - Terpineol
No. 48A
Approximate
Level
(ppb)
1
1
1
1
1
-------
85
TABLE B151
Organic Compounds Identified in Base Extract of Sample No.48B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.593 C15 Terpineol 1
TABLE B152
Volatile Organic Compounds Identified in Sample No. 49S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.631
1.000
1.508
1.934
1.986
Compound
Freon-11
Chloroform
Trichloroethylene
Trichloropropane
Tetrachloroethylene
Approximate
Level
(ppb)
1
2
1
2
1
-------
86
TABLE B153
Organic Compounds Identified in Acid Extract of Sample No. 49A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.438
1.000
1.101
1.232
1.279
1.336
1.403
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Wz
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C15 - Terpineol
Approximate
Level
(ppb)
_ _ _
3
4
2
3
1
1
TABLE B154
Organic Compounds Identified in Base Extract of Sample No. 49B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.025 Dibutyl Phthalate 1
3 2.478 Diethyl Hexyl Phthalate 2
-------
87
TABLE B155
Volatile Organic Compounds Identified in Sample No. 60S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
TABLE B156
Organic Compounds Identified in Acid Extract of Sample No. 50A
Peak
No.
1
2
3
Relative
Retention
Time
0.447
1.000
1.096
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
2
2
TABLE B157
Organic Compounds Identified in Base Extract of Sample No.508
Relstive Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.964 Dibutyl Phthalate 1
3 2.390 Diethyl Hexyl Phthalate 1
4 2.509 C15 Terpineol 1
-------
88
TABLE B158
Volatile Organic Compounds Identified in Sample No. 51S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.502
0.835
1.000
1.101
1.233
1.302
1.429
1.514
1.559
1.779
1.928
2.007
2.108
Compound
Acetone
Tetrahydrofuran
Chloroform
Pentane
Carbon Tetrachloride
Bromo-Dichloromethane
?
Trichloroethylene
Di bromo-Chl oromethane
Tribromomethane
Bromobenzene
Tetrachloroethylene
Toluene
TABLE B159
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
Relative
Retention
Time
0.454
1.000
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Approximate
Level
(ppb)
3
1
47
1
2
10
4
1
6
1
38
2
1
of Sample No. 51A
Approximate
Level
(ppb)
-
1
-------
89
TABLE B160
Organic Compounds Identified in Base Extract of Sample No.51B
Peak
No.
1
2
Peak
No.
1
2
3
Relative
Retention
Time
1.000
2.460
Volatile
Relative
Retention
Time
1.000
1.496
1.986
Compound
Camphor (IS)
Diethyl Hexyl Phthalate
TABLE B161
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Tetrachloroethylene
TABLE B162
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.445
1.000
1 . 1 03
1.247
1.343
1.409
1.461
1.552
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Pa Imitate
Methyl Stearate
Dioctyl Adipate
Diethyl Hexyl Phthalate
C,5 - Terpineol
?
?
Approximate
Level
(ppb)
___
1
52S
Approximate
Level
(ppb)
2
2
2
No. 52A
Approximate
Level
(ppb)
_
4
4
2
1
2
1
1
-------
90
TABLE B163
Organic Compounds Identified in Base Extract of Sample No.52B
Peak
No.
1
2
3
4
5
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Relative
Retention
Time
1.000
1.556 .
2.089
2.564
2.693
Volatile
Relative
Retention
Time
0.538
0.769
0.895
0.963
1.000
1.084
1.220
1.288
1.425
1.493
1.530
1.666
1.750
1.960
2.086
Compound
Camphor (IS)
C,0 Terpineol
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,5 - Terpineol
TABLE B164
Organic Compounds Identified in Sample No.
Compound
Acetone
Dimethoxymethane
2-Methyl Propanal
1 ,2-Dichloroethane
Chloroform
1 ,2-Dichloroethane
Carbon Tetrachloride
Bromo-Di chl oromethane
?
Trichloroethylene
Di bromo-Chl oromethane
Dichloro-Iodomethane
Tribromomethane
Dichlorobenzene
Dichlorobenzene
Approximate
Level
(ppb)
_
1
1
2
1
53S
Approximate
Level
(ppb)
1
8
1
4
68
4
1
12
1
1
10
1
1
10
15
-------
91
TABLE B165
Organic Compounds Identified in Acid Extract of Sample No. 53A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.450
1.000
1.338
1.409
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Diethyl Hexyl Phthalate
C15 - Terpineol
TABLE B166
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
4
5
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.658
2.053
2.511
2.643
Volatile
Relative
Retention
Time
1.000
1.516
1.559
Compound
Camphor (IS)
C,Q Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
C,r Terpineol
TABLE B167
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Benzene
Approximate
Level
(ppb)
1
1
1
No.538
Approximate
Level
(ppb)
...
3
1
2
2
54S
Approximate
Level
(ppb)
1
2
1
-------
92
TABLE B168
Organic Compounds Identified in Acid Extract of Sample No. 54A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.450
1.000
1.103
1.342
1.409
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, 5 - Terpineol
TABLE B169
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
Peak
No.
1
2
3
Relative
Retention
Time
1.000
2.053
2.505
Volatile
Relative
Retention
Time
1.000
1.488
1.965
Compound
Camphor (IS)
Di butyl Phthalate
Diethyl Hexyl Phthalate
TABLE B170
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Tetrachloroethylene
Approximate
Level
(ppb)
_ _ _
1
1
1
1
No. 54B
Approximate
Level
(ppb)
_
1
1
55S
Approximate
Level
(ppb)
2
1
1
-------
93
TABLE B171
Organic Compounds Identified in Acid Extract of Sample No. 55A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.450
1.000
1.097
1.332
1.398
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, c - Terpineol
Approximate
Level
(ppb)
_ _ _
1
2
1
1
TABLE B172
Organic Compounds Identified in Base Extract of Sample No. 55B
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.955
2.373
Compound
Camphor (IS)
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
TABLE B173
Volatile Organic Compounds Identified in Sample No. 56S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.531 Trichloroethylene 1
3 2.040 Tetrachloroethylene 1
-------
94
TABLE B174
Organic Compounds Identified in Acid Extract of Sample No.56A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.432
1.000
1.097
1.333
1.400
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C,r - Terpineol
TABLE B175
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
4
Peak
No.
1
2
3
Relative
Retention
Time
1.000
2.048
2.506
2.637
Volatile
Relative
Retention
Time
1.000
1.493
1.966
Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,r Terpineol
TABLE B176
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
_ _ _
3
2
1
1
No. 56B
Approximate
Level
(ppb)
...
2
2
2
57 S
Approximate
Level
(ppb)
1
2
2
-------
95
TABLE B177
Organic Compounds Identified in Acid Extract of Sample No. 57A
Peak
No.
1
2
3
Relative
Retention
Time
0.439
1.000
1.097
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl S tea rate
Approximate
Level
(ppb)
___
5
5
TABLE 8178
Organic Compounds Identified in Base Extract of Sample No. 578
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.885
2.570
Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
1
1
TABLE B179
Volatile Organic Compounds Identified in Sample No.58S
Peak
No.
1
2
Relative
Retention
Time
0.499
1.000
Compound
Acetone
Chloroform
Approximate
Level
(ppb)
1
3
-------
96
TABLE B180
Organic Compounds Identified in Acid Extract of Sample No. 58A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.415
0.890
1.000
1.098
1.137
1.404
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C15 - Terpineol
TABLE B181
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
Peak
No.
1
2
Relative
Retention
Time
1.000
1.807
2.442
Volatile
Relative
Retention
Time
1.000
1.937
Compound
Camphor (IS)
?
Diethyl Hexyl Phthalate
TABLE B182
Organic Compounds Identified in Sample No.
Compound
Chloroform
Bromobenzene
Approximate
Level
(ppb)
___
1
4
4
1
1
No. 58B
Approximate
Level
(ppb)
_
1
2
59S
Approximate
Level
(ppb)
1
3
-------
97
TABLE B183
Organic Compounds Identified in Acid Extract of Sample No. 59A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.393
1.000
1.102
1.334
1.400
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C-,r - Terpineol
Approximate
Level
(ppb)
_ _
4
3
2
2
TABLE B184
Organic Compounds Identified in Base Extract of Sample No. 59B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.047 Dibutyl Phthalate 3
3 2.505 Diethyl Hexyl Phthalate 1
4 2.632 C.,. Terpineol 1
I 3
-------
98
TABLE B185
Volatile Organic Compounds Identified in Sample No. 60S
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.471
1.000
1.124
1.304
1.343
1.484
1.575
1.619
1.642
2.216
Compound
Acetone
Chloroform
Pentane
Ethyl Acetate
Bromo-Dichloromethane
Dichloropropane
Trichloroethylene
Benzene
Di bromo-Chl oromethane
Toluene
Approximate
Level
(ppb)
1
30
2
1
5
1
1
1
1
2
TABLE B186
Organic Compounds Identified in Acid Extract of Sample No. 60A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.442
1.000
1.103
1.343
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
4
3
1
-------
99
TABLE B187
Organic Compounds Identified in Base Extract of Sample No.60B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.517 C]0 Terpineol 1
3 2.477 Diethyl Hexyl Phthalate 1
TABLE B188
Volatile Organic Compounds Identified in Sample No. 61S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.519 Trichloroethylene 1
3 1.696 Hexane 1
-------
100
TABLE B189
Organic Compounds Identified in Acid Extract of Sample No. 61A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.450
1.000
1.097
1.266
1.278
1.308
1.339
1.360
1.387
1.442
1.481
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Methyl Dihydroabietate
Fatty Acid Methyl Ester C >_ 22
Hydrocarbon C > 26
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C _> 24
Hydrocarbon C > 28
Fatty Acid Methyl Ester C >_ 26
Hydrocarbon C > 8
Approximate
Level
(ppb)
_ _ _
4
4
3
3
2
2
5
3
8
4
-------
101
TABLE B190
Organic Compounds Identified in Base Extract of Sample No.61B
Peak
No.
1
2
3
4
5
6
7
8
9
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
1.000
1.903
2.059
2.203
2.266
2.537
2.583
2.594
2.669
Volatile
Relative
Retention
Time
0.864
1.000
1.082
1.187
1.537
1.936
2.007
2.045
Compound
Camphor (IS)
Anthracene
Di butyl Phthalate
C16H10
C16H10
Diethyl Hexyl Phthalate
C18H12
C18H12
C,r Terpineol
TABLE B191
Organic Compounds Identified in Sample No.
Compound /
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Bromo-Dichloromethane
Trichloroethylene
4-Methyl-2-Ethyl-l ,3-Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrach 1 oroethyl ene
Approximate
Level
(ppb)
___
1
1
2
3
2
1
1
1
62S
Approximate
Level
(ppb)
3
4
10
2
2
1
1
2
-------
102
TABLE B192
Organic Compounds Identified in Acid Extract of Sample No.62A
Peak
No.
1
2
3
5
6
7
8
9
10
Relative
Retention
Time
0.442
0.894
0.948
1.000
1.070
1.206
1.282
1.343
1.412
Approximate
Level
Compound (ppb)
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Fatty Acid Methyl Ester C >_ 15
Methyl Palmitate
C,r Terpene
C,r Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
C,g - Terpineol
TABLE B193
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
2.018
2.059
2.365
2.477
2.606
Compound
Camphor (IS)
Di butyl Phthalate
Dibutyl Nonanedioate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Clf- Terpineol
6
2
16
2
7
6
2
1
No.626
Approximate
Level
(ppb)
__
2
2
3
2
1
-------
103
TABLE B194
Volatile Organic Compounds Identified in Sample No. 63S
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.872
1.000
1.075
1.368
1.506
1.895
1.970
2.007
Compound
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Bromo-Di chl oroethane
Trichloroethylene
Ethyl Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
TABLE B195
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.431
0.890
0.945
1.000
1.091
1.128
1.164
1.177
1.204
1.225
1.277
1.341
1.362
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Palmitate
Methyl Stearate
?
C, 5 Terpene
Diisobutyl Phthalate
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
Approximate
Level
(ppb)
2
6
9
9
3
1
1
2
Sample No. 63A
Approximate
Level
(ppb)
_
6
1
19
13
3
3
3
3
2
23
3
1
-------
104
TABLE B196
Organic Compounds Identified in Base Extract of Sample No. 63B
Peak
No.
1
2
3
4
5
6
Peak
No.
1
2
.3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.260
1.555
2.066
2.424
2.540
Volatile
Relative
Retention
Time
0.882
1.000
1.081
1.366
1.512
1.840
1.910
1.986
2.020
Compound
Camphor (IS)
Benzothiazole
C n Terpineol
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
TABLE B197
Organic Compounds Identified in Sample No.
Compound
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Bromo-Dichl oroethane
Trichloroethylene
?
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
-
6
1
1
4
2
64S
Approximate
Level
(ppb)
4
10
8
1
4
1
1
1
2
-------
105
TABLE B198
Organic Compounds Identified in Acid Extract of Sample No. 64A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.416
0.887
1.000
1.091
1.198
1.219
1.271
1.341
1.411
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myrsitate
Methyl Palmitate
Methyl Stearate
C Terpene
?
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C, 5 - Terpineol
Approximate
Level
(ppb)
2
6
4
3
1
1
2
1
TABLE B199
Organic Compounds Identified in Base Extract of Sample No. 64B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.286 Benzothiazole 2
3 1.549 C,Q Terpineol 1
4 2.053 Dibutyl Phthalate 1
5 2.523 Diethyl Hexyl Phthalate 1
6 2.654 C,5 Terpineol 1
-------
106
TABLE B200
Volatile Organic Compounds Identified in Sample No. 65S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Relative
Retention
Time
0.456
0.876
0.957
1.000
1.086
1.193
1.382
1.431
1.522
1.678
1.792
1.846
1.921
1.991
2.028
Compound
Dichloromethane
Tetrahydrofuran
1 ,2-Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Bromo-Chloroethane
1 ,2-Dichloropropane
Trichloroethylene
1 -Bromo-2-Chl oropropane
Tribromomethane
?
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
TABLE B201'
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.434
1.000
1.097
1.228
1.280
1.341
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
?
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
15
3
20
9
2
1
1
8
2
2
2
8
3
6
Sample No. 65A
Approximate
Level
(ppb)
_ _ _
3
3
1
1
2
-------
107
TABLE B202
Organic Compounds Identified in Base Extract of Sample No. 65B
Peak
No.
1
2
3
4
5
6
7
8
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
1.000
1.177
1.544
1.595
1.744
1.876
2.047
2.511
Volatile
Relative
Retention
Time
0.451
0.877
0.957
1.000
1.085
1.186
1.506
1.655
1.773
1.826
1.895
1.970
2.007
Compound
Camphor (IS)
Bromopropyl Benzene
C22H14
?
C,n Camphenol
C,Q Camphenol
Dibutyl Phthalate
Di ethyl Hexyl Phthalate
TABLE B203
Organic Compounds Identified in Sample No.
Compound
Dichloromethane
Tetrahydrofuran
1 ,2-Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 -Chi oro-2-Bromopropane
Tribromomethane
?
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
Approximate
Level
(ppb)
_
3
2
3
2
2
1
1
66S
Approximate
Level
(ppb)
2
15
2
14
9
1
8
1
1
1
12
2
6
-------
108
TABLE B204
Organic Compounds Identified in Acid Extract of Sample No. 66A
Peak
No.
1
2
.3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Relative
Retention
Time
0.429
0.670
0.890
0.900
0.920
0.948
0.969
1.000
1.009
1.058
1.101
1.207
1.231
1.281
1.345
1.369
1.415
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloroanisole
Methyl Myri state
Methyl Dichlorophenoxy Acetate
Methyl Dichlorophenoxy Acetate
Pentachloroanisole
Methyl -2 (4-chlorophenoxy)Butanoate
Methyl Palmitate
Cnr Terpene
?
Methyl Stearate
C, 5 Terpene
?
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
?
C,c - Terpineol
Approximate
Level
(ppb)
_ _
1
3
1
1
1
2
8
2
2
5
3
3
19
2
2
2
TABLE B205
Organic Compounds Identified in Base Extract of Sample No. 66B
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.552
1.604
2.069
2.424
2.540
Compound
Camphor (IS)
C5H10C12
?
Di butyl Phthalate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
2
1
2
10
1
-------
109
TABLE B206
Volatile Organic Compounds Identified in Sample No. 67S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.459
0.882
1.000
1.075
1.182
1.509
1.662
1.777
1.991
1.986
2.018
Compound
Dichloromethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 -Chi oro-2-Bromoethane
Tribromomethane
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
TABLE B207
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.440
0.897
0.953
1.000
1.051
1.097
1.328
1.393
1.460
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Palmitate
?
Methyl Stearate
Diethyl Hexyl Phthalate
C,5 Terpineol
?
Approximate
Level
(ppb)
2
5
6
8
1
8
3
1
4
6
9
Sample No. 67A
Approximate
Level
(ppb)
1
1
10
1
10
2
1
1
-------
no
TABLE B208
Organic Compounds Identified in Base Extract of Sample No.67B
Peak
No.
1
2
3
4
5
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
1.000
2.562
2.688
2.821
2.975
Volatile
Relative
Retention
Time
0.439
0.881
0.951
1.000
1.035
1.183
1.512
1.975
2.002
2.056
2.179
Compound
Camphor (IS)
Diethyl Hexyl Phthalate
C-|5 Terpineol
?
?
TABU B^oy
Organic Compounds Identified in Sample No.
Compound
Dichloromethane
Tetrahydrofuran
1,2-Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1,1-Trichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
Dichlorobenzene
Dichlorobenzene
Approximate
Level
(ppb)
___
2
1
1
1
68S
Approximate
Level
(ppb)
2
1
2
4
1
1
4
1
4
8
8
-------
Ill
TABLE B210
Organic Compounds Identified in Acid Extract of Sample No. 68A
Peak
No.
1
2
3
4
5
5
6
Relative
Retention
Time
0.422
0.800
0.867
1.000
1.027
1.068
1.301
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
Methyl Myri state
Methyl Palmitate
?
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
1
2
6
1
5
3
TABLE B211
Organic Compounds Identified in Base Extract of Sample No. 68B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.646 Unidentified Phthalate 1
3 2.024 Dibutyl Phthalate 1
4 2.439 Diethyl Hexyl Phthalate 1
5 2.576 C 5 Terpineol 1
6 2.713 ? 1
7 2.861 ? 2
-------
112
TABLE B212
Volatile Organic Compounds Identified in Sample No. 69S
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.442
0.881
1.000
1.081
1.184
1.509
1.975
2.013
Compound
Dichloromethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
TABLE B213
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.450
0.800
0.900
1.000
1.062
1.102
1.204
1.264
1.279
1.339
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
Methyl Myri state
Methyl Palmitate
Hydrocarbon C > 18
Methyl Stearate
C,5 Terpene
Hydrocarbon C > 24
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
12
3
3
10
9
8
Sample No. 69A
Approximate
Level
(ppb)
2
4
11
2
9
3
2
2
2
-------
113
TABLE B214
Organic Compounds Identified in Base Extract of Sample No. 69B
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
2.027
2.463
2.593
2.675
2.720
2.897
Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,5 Terpineol
Hydrocarbon C ^ 30
?
?
Approximate
Level
(ppb)
___
1
1
1
1
2
2
TABLE B215
Volatile Organic Compounds Identified in Sample No. 70S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.080 1,2-Dichloroethane 2
3 1.514 Trichloroethylene 2
4 2.018 Tetrachloroethylene 4
-------
114
TABLE B216
Organic Compounds Identified in Acid Extract of Sample No. 70A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.445
0.533
0.895
0.952
1.000
1.036
1.054
1.105
1.129
1.207
1.219
1.228
1.249
1.270
1.285
1.355
1.432
1.456
1.526
1.559
Compound
Methyl -2-Ethyl Hexanoate (IS)
Hexachlorobutadiene
Methyl Myri state
Pentachloroanisole
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
Fatty Acid Methyl Ester C 1 16
Methyl Stearate
?
C,r Terpene
?
Hydrocarbon C >_ 22
Dioctyl Adi pate
Hydrocarbon C > 22
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Hydrocarbon C > 26
?
Hydrocarbon C > 28
Hydrocarbon C > 30
Approximate
Level
(ppb)
V _
1
9
2
28
5
7
29
17
7
7
9
20
9
12
1264
13
43
14
21
-------
115
TABLE B217
Organic Compounds Identified in Base Extract of Sample No. 70B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
Relative
Retention
Time
0.803
1.000
1.028
1.517
1.539
1.630
1.730
1.786
1.865
1.910
1.938
2.051
2.118
2.160
2.200
2.260
2.290
2.326
2.360
2.398
2.472
2.635
2.685
2.730
2.815
2.854
2.882
2.921
Compound
Hexachloroethane
Camphor (IS)
Hexachlorobutadiene
Hydrocarbon C >_ 14
Hydrocarbon C ^ 14
Hydrocarbon C >_ 16
Hydrocarbon C >_ 16
Hydrocarbon C >_ 18
Hydrocarbon C >_ 18
Hydrocarbon C >_ 18
Hydrocarbon C > 18
Di butyl Phthalate
Hydrocarbon C >_ 20
Unidentified Phthalate
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
Dioctyl Adi pate
Hydrocarbon C >_ 22
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Hydrocarbon C ^ 30
?
Hydrocarbon C ^ 30
Unidentified Phthalate
Hydrocarbon C >_ 30
Hydrocarbon C ^ 30
?
Approximate
Level
(ppb)
1
1
9
13
12
11
6
11
8
16
14
21
4
8
4
4
14
3
14
2347
13
65
200
7
34
13
92
-------
116
TABLE B218
Volatile Organic Compounds Identified in Sample No. 71S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.067.
1.444
1.893
1.924
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
2
2
3
1
3
-------
117
TABLE B219
Organic Compounds Identified in Acid Extract of Sample No. 71A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.428
0.778
0.820
0.892
0.931
0.946
1.000
1.039
1.051
1.096
1.201
1.245
1.275
1.305
1.335
1.356
1.374
1.400
1.476
1.559
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
C,Q Terpineol
Methyl Myri state
Fatty Acid Methyl Ester C i 14
Pentachloroanisole
Methyl Palmitate
Unidentified Phthalate
Fatty Acid Methyl Ester C 1 16
Methyl Stearate
C.c Terpene
1 b
Dioctyl Adi pate
Butyl Phthalyl Butyl Glycolate
Butyl Benzyl Phthalate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 22
Dioctyl Phthalate
C,,- Terpineol
?
?
Approximate
Level
(ppb)
___
2
2
3
1
1
9
1
1
11
1
2
2
1
2
2
2
3
2
6
-------
118
TABLE B220
Organic Compounds Identified in Base Extract of Sample No. 71B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
Relative
Retention
Time
1.000
1.508
1.610
1.708
1.805
1.903
2.000
2.038
2.060
2.069
2.157
2.238
2.270
2.314
2.335
2.384
2.438
2.459
2.508
2.529
2.562
2.600
2.638
2.670
2.692
2.746
2.784
2.843
Compound
Camphor (IS)
C,Q Terpineol
Hydrocarbon C >_ 14
Hydrocarbon C >_ 16
Hydrocarbon C ^ 16
Diisobutyl Phthalate
Dibutyl Phthalate
Diisobutyl Nonanedioate
?
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
Hydrocarbon C >_ 22
Dioctyl Adi pate
Hydrocarbon C >_ 22
?
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Hydrocarbon C >_ 24
Dicyclohexyl Phthalate
Hydrocarbon C >_ 26
C-.C- Terpineol
Hydrocarbon C ^ 26
?
Hydrocarbon C >_ 28
?
Hydrocarbon C >_ 28
Hydrocarbon C >_ 28
?
Approximate
Level
(ppb)
___
3
3
3
3
9
20
4
8
5
6
9
10
5
4
15
19
5
7
5
12
5
6
4
8
7
7
20
-------
119
TABLE B221
Volatile Organic Compounds Identified in Sample No. 72S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.081
1.514
1.986
2.018
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
2
2
2
1
2
TABLE B222
Organic Compounds Identified in Acid Extract of Sample No. 72A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.437
0.882
0.895
1.000
1.099
1.277
1.337
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
2
3
1
1
-------
120
TABLE B223
Organic Compounds Identified in Base Extract of Sample No. 72B
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.525
2.034
2.374
2.486
2.620
Compound
Camphor (IS)
C,Q - Terpineol
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C-|5 Terpineol
Approximate
Level
(ppb)
- _ _
1
3
3
33
3
TABLE B224
Volatile Organic Compounds Identified in Sample No. 73S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.075 1,2-Dichloroethane 1
3 1.504 Trichloroethylene 1
4 2.007 Tetrachloroethylene 1
-------
121
TABLE B225
Organic Compounds Identified in Acid Extract of Sample No. 73A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.433
0.780
0.819
0.894
1.000
1.096
1.338
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
C, Q Terpineol
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
__
3
6
2
7
5
1
TABLE B226
Organic Compounds Identified in Base Extract of Sample No. 73B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.517 C]0 Terpineol 1
3 2.018 Dibutyl Phthalate 1
4 2.463 Diethyl Hexyl Phthalate 1
-------
122
TABLE B227
Volatile Organic Compounds Identified in Sample No. 74S
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.080
1.996
Compound
Chloroform
1 ,2-Dichloroethane
Tetrachloroethylene
Approximate
Level
(ppb)
2
2
1
TABLE B228
Organic Compounds Identified in Acid Extract of Sample No. 74A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.435
0.813
1.000
1.098
1.330
1.402
Compound
Methyl -2-Ethyl Hexanoate (IS)
C, 0 Terpineol
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C,r Terpineol
Approximate
Level
(ppb)
___
3
4
3
5
1
-------
123
TABLE B229
Organic Compounds Identified in Base Extract of Sample No. 74B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.511 CIQ Terpineol 2
TABLE B230
Volatile Organic Compounds Identified in Sample No. 75S
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.095
1.330
1.615
2.009
2.103
2.259
Compound
Chloroform
1 ,2-Dichloroethane
Bromo-Dichloromethane
Di bromo-Chl oromethane
Dichlorobenzene
Toluene
Dichlorobenzene
Approximate
Level
(ppb)
22
2
4
1
1
1
1
-------
124
TABLE B231
Organic Compounds Identified in Acid Extract of Sample No. 75A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.440
0.816
1.000
1.039
1.103
1.139
1.184
1.226
1.269
1.281
1.311
1.341
1.389
1.407
Compound
Methyl -2-Ethyl Hexanoate (IS)
C-.Q Terpineol
Methyl Palmitate
Hydrocarbon C > 18
Methyl Stearate
Hydrocarbon C > 20
Hydrocarbon C > 20
Hydrocarbon C > 22
Hydrocarbon C > 22
Butyl Phthalyl Butyl Glycolate
Hydrocarbon C > 24
Di ethyl Hexyl Phthalate
Hydrocarbon C >_ 26
C, [- Terpineol
Approximate
Level
(ppb)
__
2
6
1
4
1
1
1
1
1
1
1
1
1
TABLE B232
Organic Compounds Identified in Base Extract of Sample No. 75B
Relative Approximate
Peak Retention . Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.521 C,Q Terpineol 2
3 2.000 Dibutyl Phthalate 1
4 2.486 Diethyl Hexyl Phthalate 1
-------
125
TABLE B233
Volatile Organic Compounds Identified in Sample No. 76S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.554 Trichloroethylene 1
TABLE B234
Organic Compounds Identified in Acid Extract of Sample No. 76A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.440
0.817
0.898
1.000
1.099
1.347
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
.
2
1
3
3
3
-------
126
TABLE B235
Organic Compounds Identified in Base Extract of Sample No. 76B
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.521
2.020
2.459
2.620
2.711
2.859
Compound
Camphor (IS)
C,n - Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
C,5 - Terpineol
?
?
Approximate
Level
(ppb)
_ _
4
1
1
1
2
2
TABLE B236
Volatile Organic Compounds Identified in Sample No. 77S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 15
2 1.562 Trichloroethylene 1
-------
127
TABLE B237
Organic Compounds Identified in Acid Extract of Sample No. 77A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.432
0.780
0.893
1.000
1.098
1.333
1.399
1.467
1.535
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, ,- Terpineol
?
?
Approximate
Level
(ppb)
___
2
2
4
3
1
1
1
1
TABLE B238
Organic Compounds Identified in Base Extract of Sample No. 77B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.543 C,Q - Terpineol 1
3 2.054 Dibutyl Phthalate 1
4 2.508 Diethyl Hexyl Phthalate 1
5 2.766 ? 1
6 2.900 ? 2
-------
128
TABLE B239
Volatile Organic Compounds Identified in Sample No. 78S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.076
1.519
1.959
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachloroethylene
Approximate
Level
(ppb)
10
5
3
2
TABLE B240
Organic Compounds Identified in Acid Extract of Sample No. 78A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.412
1.000
1.103
1.339
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
...
2
2
1
TABLE B241
Organic Compounds Identified in Base Extract of Sample No. 78B
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.548
2.062
2.508
Compound
Camphor (IS)
C,Q - Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
1
-------
129
TABLE B242
Volatile Organic Compounds Identified in Sample No. 79S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.975 Dichlorobenzene 3
TABLE B243
Organic Compounds Identified in Acid Extract of Sample No. 79A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.435
0.816
1.000
1.098
1.321
Compound
Methyl -2-Ethyl Hexanoate (IS)
C, Q Terpineol
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
1
2
2
1
TABLE B244
Organic Compounds Identified in Base Extract of Sample No. 79B
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.516
2.027
2.457
Compound
Camphor (IS)
C,Q - Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
3
1
1
-------
130
TABLE B245
Volatile Organic Compounds Identified in Sample No. 80S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
TABLE B246
Organic Compounds Identified in Acid Extract of Sample No. 80A
Peak
No.
1
2
.3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.435
0.818
0.869
0.922
0.976
1.000
1.027
1.078
1.093
1.164
1.206
1.248
1.343
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
C-.,- Alcohol
C,c Alcohol
1 b
C,y Alcohol
Methyl Palmitate
C,g Alcohol
C,g Alcohol
Methyl Stearate
C2Q Alcohol
C_, Alcohol
C22 Alcohol
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
4
4
3
1
5
1
1
3
1
1
1
1
-------
131
TABLE B247
Organic Compounds Identified in Base Extract of Sample No. SOB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.667 Diethyl Hexyl Phthalate 1
3 2.800 C]5 - Terpineol 1
4 2.981 ? 1
5 3.095 ? 1
TABLE B248
Volatile Organic Compounds Identified in Sample No. 81S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 14
2 1.528 Trichloroethylene 2
-------
132
TABLE B249
Organic Compounds Identified in Acid Extract of Sample No. 81A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.450
1.000
1.098
1.260
1.328
1.396
1.461
1.541
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Methyl Dehydroabietate
Di ethyl Hexyl Phthalate
C, (- Terpineol
1 0
?
?
Approximate
Level
(ppb)
_ _ _
4
3
1
1
1
1
1
TABLE B250
Organic Compounds Identified in Base Extract of Sample No. 81B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.508 Diethyl Hexyl Phthalate 1
3 2.635 C15 ~ TerPineo1 1
4 2.773 ? 4
5 2.945 ? 3
-------
133
TABLE B251
Volatile Organic Compounds Identified in Sample No. 82S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 12
TABLE B252
Organic Compounds Identified in Acid Extract of Sample No. 82A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.345
1.000
1.101
1.348
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
2
4
TABLE B253
Organic Compounds Identified in Base Extract of Sample No. 82B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.565 CIQ - Terpineol 1
3 2.102 Dibutyl Phthalate 1
4 2.579 Diethyl Hexyl Phthalate 1
-------
134
TABLE B254
Volatile Organic Compounds Identified in Sample No. 83S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.500 Trichloroethylene 2
TABLE B255
Organic Compounds Identified in Acid Extract of Sample No. 83A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.424
0.819
0.890
1.000
1.104
1.347
1.415
Compound
Methyl -2-Ethyl Hexanoate (IS)
CIQ Terpineol
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C15 Terpineol
Approximate
Level
(ppb)
2
1
5
4
1
1
-------
135
TABLE B256
Organic Compounds Identified in Base Extract of Sample No. 83B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.528 Diethyl Hexyl Phthalate 1
TABLE B257
Volatile Organic Compounds Identified in Sample No. 84S
Peak
No.
1
2
Relative
Retention
Time
1.000
1.498
Compound
Chloroform
Trichloroethylene
Approximate
Level
(Ppb)
1
1
TABLE B258
Organic Compounds Identified in Acid Extract of Sample No. 84A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.430
1.000
1.105
1.354
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
2
1
-------
136
TABLE B259
Organic Compounds Identified in Base Extract of Sample No. 84B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B260
Volatile Organic Compounds Identified in Sample No. 85S
Peak
No.
1
2
.3
4
5
6
7
Relative
Retention
Time
0.958
1.000
1.078
1.182
1.506
1.980
2.017
Compound
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
1
2
1
1
3
1
3
-------
137
TABLE B261
Organic Compounds Identified in Acid Extract of Sample No. 85A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.400
1.000
1.100
1.347
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
4
5
2
TABLE B262
Organic Compounds Identified in Base Extract of Sample No. 85B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.558 C]0 - Terpineol 2
3 2.024 Diphenyl Benzene 1
4 2.070 Dibutyl Phthalate 1
5 2.536 Diethyl Hexyl Phthalate 2
-------
138
TABLE B263
Volatile Organic Compounds Identified in Sample No. 86S
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.431
0.879
0.953
1.000
1.079
1.184
1.511
1.991
2.028
Compound
Dichloromethane
Tetrahydrofuran
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1,1,1 -Tr i chl oroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
1
1
1
10
1
1
5
3
12
-------
139
TABLE B264
Organic Compounds Identified in Acid Extract of Sample No. 86A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time
0.419
0.666
0.766
0.888
0.899
0.927
0.967
1.000
1.061
1.103
1.139
1.207
1.234
1.271
1.350
1.416
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloroanisole
Methyl Laurate
Methyl Myri state
Methyl Dichlorophenoxy Acetate
Methyl Dichlorophenoxy Acetate
Methyl -Trichlorophenoxy Acetate
Methyl Palmitate
?
Methyl Stearate
Diphenyl Sulfone
C16H10
?
Methyl Dehydroabietate
Di ethyl Hexyl Phthalate
C, 5 Terpineol
Approximate
Level
(ppb)
_ _ _
1
1
5
6
5
5
10
2
11
4
8
6
5
24
1
-------
140
TABLE B265
Organic Compounds Identified in Base Extract of Sample No. 86B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.574
1.734
2.013
2.119
2.208
2.552
2.611
2.741
2.877
3.049
Volatile
Relative
Retentioa
Time
1.000
1.084
1.511
2.027
Compound
Camphor (IS)
C,0 - Terpineol
Diethyl Phthalate
Diisobutyl Phthalate
Di butyl Phthalate
?
Unidentified Phthalate
Diethyl Hexyl Phthalate
C,5 - Terpineol
?
?
TABLE B266
Organic Compounds Identified in Sample No.
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachloroethylene
Approximate
Level
(ppb)
_ _ _
4
5
4
5
2
1
15
1
2
5
87S
Approximate
Level
(ppb)
4
1
1
1
-------
141
TABLE B267
Organic Compounds Identified in Acid Extract of Sample No. 87A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.425
0.765
0.814
0.887
0.945
1.000
1.104
1.351
1.421
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
C, 0 Terpineol
Methyl Myri state
Pentachloroanisole
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C15 Terpineol
Approximate
Level
(ppb)
___
1
2
1
1
8
8
1
1
TABLE B268
Organic Compounds Identified in Base Extract of Sample No. 87B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.071 Dibutyl Phthalate 1
3 2.562 Diethyl Hexyl Phthalate 10
4 2.828 ? 2
5 2.990 ? 2
-------
142
TABLE B269
Volatile Organic Compounds Identified in Sample No. 88S
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.456
0.954
1.000
1.483
1.777
1.970
Compound
Dichloromethane
Dichloroethylene
Chloroform
Trichloroethylene
Bromobenzene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
1
1
8
10
7
2
TABLE B270
Organic Compounds Identified in Acid Extract of Sample No. 88A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.425
1.000
1.099
1.268
1.341
1.410
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Methyl Dehydroabietate
Di ethyl Hexyl Phthalate
C, 5 Terpineol
Approximate
Level
(ppb)
___
2
1
4
1
1
-------
143
TABLE B271
Organic Compounds Identified in Base Extract of Sample No.
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
2.539
2.636
2.676
Compound
Camphor (IS)
Diethyl Hexyl Phthalate
Hydrocarbon C >_ 26
C,r - Terpineol
Approximate
Level
(ppb)
1
2
2
TABLE B272
Volatile Organic Compounds Identified in Sample No. 89S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.927 Dichloroethylene 1
2 1.000 Chloroform 4
3 1.084 1,2-Dichloroethane 1
4 1.138 Pentane 1
5 1.222 Cyclohexane 1
6 1.576 Trichloroethylene 1
7 2.128 Tetrachloroethylene 1
8 2.382 Dichlorobenzene 12
-------
144
TABLE B273
Organic Compounds Identified in Acid Extract of Sample No. 89A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.408
0.851
0.888
1.000
1.103
1.348
1.417
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, 5 Terpineol
Approximate
Level
(ppb)
___
1
1
3
2
1
1
TABLE B274
Organic Compounds Identified in Base Extract of Sample No.89B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.639 Diethyl Hexyl Phthalate 1
-------
145
TABLE B275
Volatile Organic Compounds Identified in Sample No.90S
Peak
No.
1
2
Relative
Retention
Time
1.000
1.136
Compound
Chloroform
Pentane
Approximate
Level
(ppb)
1
1
TABLE B276
Organic Compounds Identified in Acid Extract of Sample No.90A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.402
1.000
1.108
1.354
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
5
3
1
TABLE B277
Organic Compounds Identified in Base Extract of Sample No.90B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.125 Dibutyl Phthalate 3
3 2.617 Diethyl Hexyl Phthalate 2
4 2.253 C]5 - Terpineol 2
-------
146
TABLE B278
Volatile Organic Compounds Identified in Sample No. 91S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.195 Cyclohexane 1
3 1.663 Hexane 1
TABLE B279
Organic Compounds Identified in Acid Extract of Sample No. 91A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.361
1.000
1.012
1.106
1.119
1.213
1.353
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
C,5 Terpene
Methyl Stearate
C,c Terpene
C,5 Terpene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
__ _
5
2
8
2
1
1
-------
147
TABLE B280
Organic Compounds Identified in Base Extract of Sample No. 91B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.594 Diethyl Hexyl Phthalate 1
3 2.728 C]5 - Terpineol 2
TABLE B281
Volatile Organic Compounds Identified in Sample No. 92S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 31
2 1.214 Cyclohexane 2
3 1.573 Trichloroethylene 1
-------
148
TABLE B282
Organic Compounds Identified in Acid Extract of Sample No. 92A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.400
1.000
1.102
1.121
1.210
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
C,r Terpene
TABLE B283
Organic Compounds Identified in Base Extract
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
2.111
2.595
2.734
Volatile
Relative
Peak Retention
. No. Time
1
1.212
Compound
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
C,r - Terpineol
/
TABLE B284
Organic Compounds Identified in
Compound
Cyclohexane
Approximate
Level
(ppb)
4
2
2
1
of Sample No. 92B
Approximate
Level
(ppb)
1
1
1
Sample No. 93S
Approximate
Level
(ppb)
1
-------
149
TABLE B285
Organic Compounds Identified in Acid Extract of Sample No. 93A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.399
0.888
1.000
1.015
1.104
1.121
1.212
1.348
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
C,,- Terpene
Methyl Stearate
C,r Terpene
C,r Terpene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
8
1
2
3
4
1
TABLE B286
Organic Compounds Identified in Base Extract of Sample No.93B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
2
3
4
5
6
1.000
1.294
1.413
1.531
.2.527
2.651
Camphor (IS)
C,,- Hydrocarbon 1
C g Hydrocarbon 1
C,7 Hydrocarbon 1
Diethyl Hexyl Phthalate 1
C15 - Terpineol 1
-------
150
TABLE B'287
Volatile Organic Compounds Identified in Sample No. 94S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.211
1.349
2.007
Compound
Chloroform
Cyclohexane
Bromo-Dichl
Toluene
+ 1 ,1 ,1-Trichloroethane
oromethane
Approximate
Level
(ppb)
30
1
3
1
TABLE B288
Organic Compounds Identified in Acid Extract of Sample No. 94A
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.229
0.341
0.400
0.416
0.498
0.688
0.752
0.816
1.000
1.351
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
Dichlorobutane
Trichloropentane
C,,- Hydrocarbon
C,g Hydrocarbon
C,7 Hydrocarbon
Methyl Palmitate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
3
1
1
1
1
1
1
1
1
-------
151
TABLE B289
Organic Compounds Identified in Base Extract of Sample No. 94B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.429 C,g Hydrocarbon 1
3 1.544 C,7 Hydrocarbon 1
4 2.550 Diethyl Hexyl Phthalate 1
5 2.649 C,5 Terpineol 1
TABLE B290
Volatile Organic Compounds Identified in Sample No.95S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.211 Cyclohexane + 1,1,1-Trichloroethane 1
-------
152
TABLE B291
Organic Compounds Identified in Acid Extract of Sample No.95A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.221
0.340
0.421
0.689
0.755
0.814
0.880
1.000
1.009
1.102
1.116
1.206
1.281
1 . 340
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
C-,r Hydrocarbon
C,g Hydrocarbon
C,7 Hydrocarbon
Methyl Myri state
Methyl Palmitate
C,5 Terpene
Methyl Stearate
C,5 Terpene
C,r Terpene
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
1
1
1
1
6
2
2
5
4
2
1
-------
153
TABLE B292
Organic Compounds Identified in Base Extract of Sample No.95B
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.531
2.056
2.405
.2.515
2.642
Compound
Camphor (IS)
C,7 Hydrocarbon
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
C,5 - Terpineol
Approximate
Level
(ppb)
_
1
1
1
2
1
TABLE B293
Volatile Organic Compounds Identified in Sample No. 96S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.211 Cyclohexane + 1,1,1-Trichloroethane 1
3 1.567 Trichloroethylene 13
4 2.005 Toluene 1
-------
154
TABLE B294
Organic Compounds Identified in Acid Extract of Sample No. 96A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.433
1.000
1.102
1.343
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
2
1
TABLE B295
Organic Compounds Identified in Base Extract of Sample No.96B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B296
Volatile Organic Compounds Identified in Sample No. 97S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.181 Cyclohexane 1
-------
155
TABLE B297
Organic Compounds Identified in Acid Extract of Sample No. 97A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.361
1.000
1.106
1.120
1.212
1.285
1.350
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
C,r Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
1
1
1
1
1
TABLE B298
Organic Compounds Identified in Base Extract of Sample No.97B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.125 Dibutyl Phthalate 2
3 2.493 Butyl Phthalyl Butyl Glycolate 36
4 2.617 Diethyl Hexyl Phthalate 2
5 .2.747 C ~ Terpineol 1
-------
156
TABLE B299
Volatile Organic Compounds Identified in Sample No. 98S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.175 Cyclohexane 4
TABLE B300
Organic Compounds Identified in Acid Extract of Sample No. 98A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.402
1.000
1.288
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
4
1
TABLE B301
Organic Compounds Identified in Base Extract of Sample No.98B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.615 Diethyl Hexyl Phthalate 1
3 2.752 C15 - Terpineol 1
-------
157
TABLE B302
Volatile Organic Compounds Identified in Sample No.99S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 1.174 Cyclohexane 4
TABLE B303
Organic Compounds Identified in Acid Extract of Sample No. 99A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.379
0.663
1.000
1.104
1.346
1.367
1.416
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloroanisole
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
C,5 Terpineol
Approximate
Level
(ppb)
1
3
2
1
1
1
-------
158
TABLE B304
Organic Compounds Identified in Base Extract of Sample No.99B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.530 Diethyl Hexyl Phthalate 1
3 2.657 C15 - Terpineol 1
TABLE B305
Volatile Organic Compounds Identified in Sample No. 100S
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.433
0.491
0.857
1.000
1.079 .
1.169
1.424
1.466
2.155
2.187
Compound
Ethanethiol
Acetone
Di-isopropyl Ether
Chloroform
Butanal
Cyclohexane
Dimethyl Bisulfide
Benzene + Trichloroethylene
C,Q Terpene
C,Q Terpene
Approximate
Level
(ppb)
19
1
1
46
6
2
19
1
1
85
-------
159
TABLE B306
Organic Compounds Identified in Acid Extract of Sample No.lOOA
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Relative
Retention
Time
0.610
0.662
0.670
0.752
0.770
0.802
0.811
0.871
0.886
0.907
0.931
0.943
0.976
1.985
1.000
1.033
1.051
1.099
1.138
1.150
1.156
1.171
1.186
1.201
1.210
1.224
1.236
1.275
1.305
1.311
1.326
Compound
Hydrocarbon C > 14
C15H24
Hydrocarbon C > 16
Hydrocarbon C > 16
Fatty Acid Methyl Ester C 12
Hydrocarbon C > 18
Hydrocarbon C > 18
Hydrocarbon C > 18
Fatty Acid Methyl Ester C 14
Tetrachl oroani sol e
Hydrocarbon C > 20
Fatty Acid Methyl Ester C > 15 +
Pentachloroanisole
Fatty Acid Methyl Ester C >_ 15
Hydrocarbon C ^ 20
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
Fatty Acid Methyl Ester C >_ 17
Methyl Stearate
Hydrocarbon C > 22
Fatty Acid Methyl Ester C 19
Terpene C 15
Cp-iH-pOp Methyl Pimarate Isomer
Cp-iH^oOp Methyl Pimarate Isomer
Fatty Acid Methyl Ester C 20
Cp^H-pOp Methyl Pimarate Isomer
Cp,H3pOp Methyl Pimarate Isomer
Cp-iH^pOp Methyl Pimarate Isomer
?
?
?
Fatty Acid Methyl Ester C > 23
Approximate
Level
(ppb)
1
8
1
1
1
1
5
6
7
1
1
4
2
1
34
12
7
62
13
5
5
16
27
58
18
22
36
340
5
5
8
-------
160
TABLE B306, cont.
Organic Compounds Identified in Acid Extract of Sample No.lOOA (continued)
Peak
No.
32
33
34
35
36
37
38
39
40
41
Relative
Retention
Time
1.344
1.365
1.383
1.398
1.404
1.413
1.425
1.443
1.478
1.569
Compound
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
?
?
?
Terpineol C 15
?
Fatty Acid Methyl Ester C > 26
?
CpiH32^2 Methyl Pimarate Isomer
Approximate
Level
(ppb)
18
36
16
18
18
8
10
12
5
3
-------
161
TABLE B307
Organic Compounds Identified in Base Extract of Sample No.lOOB
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Relative
Retention
Time
0.384
0.520
0.627
0.881
0.994
1.000
1.041
1.101
1.136
1.189
1.255
1.279
1.326
1.397
1.456
1.498
1.563
1.581
1.622
1.699
1.770
1.812
1.924
1.948
1.996
2.031
2.061
2.078
2.132
2.144
2.209
Compound
Diterpene C,QH,g
Diterpene C,QH,g
Diterpene C, -H, fi
Terpineol C 10
Hydroxylborneol
Camphor
Diterpene C,QH16
Dimethyl Styrene
Hydrocarbon C > 14
Hydrocarbon C > 14
Hydrocarbon C >_ 14
Triterpene C1t.H?.
Hydrocarbon C >_ 14
Triterpene C, 5H2«
Hydrocarbon C >_ 16
Hydrocarbon C > 16
Hydrocarbon C >_ 16
Hydrocarbon C >_ 16
Triterpene C, ,-H24
Hydrocarbon C ^ 18
?
Hydrocarbon C > 18
Hydrocarbon C >_ 20
Terpene C 15
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
?
?
Hydrocarbon C >_ 22
Dibutyl Phthalate
?
Approximate
Level
(ppb)
9
6
3
13
31
59
29
1
27
1
12
14
24
17
24
50
2
2
23
3
15
18
5
9
12
3
3
12
10
10
-------
162
TABLE B307, cont.
Organic Compounds Identified in Base Extract of Sample No.lOOB (continued)
Peak
No.
32
33
34
35
36
37
38
39
40
41
42
43
44
Relative
Retention
Time
2.245
2.256
2.292
2.345
2.376
2.384
2.404
2.422
2.434
2.446
2.570
2.630
2.750
Compound
Hydrocarbon C > 22
?
?
Hydrocarbon C > 24
Hydrocarbon C > 24
?
Hydrocarbon C > 24
?
?
?
Hydrocarbon C > 26
Diethyl Hexyl Phthalate
Terpineol C 15
Approximate
Level
(ppb)
3
7
2
10
7
51
3
40
4
5
3
3
3
-------
163
TABLE B308
Volatile Organic Compounds Identified in Sample No. 101S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.176 Cyclohexane 1
TABLE B309
Organic Compounds Identified in Acid Extract of Sample No.lOlA
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.412
1.000
1.103
1.212
1.288
1.352
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
5
3
1
3
1
-------
164
TABLE B310
Organic Compounds Identified in Base Extract of Sample No.lOlB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.541 Diethyl Hexyl Phthalate 1
3 2.666 C c - Terpineol 1
12 . _
TABLE B311
Volatile Organic Compounds Identified in Sample No. 102S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.265 Dioxolane 1
3 1.821 Bromobenzene 20
-------
165
TABLE B312
Organic Compounds Identified in Acid Extract of Sample No.lOZA
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.415
1.000
1.064
1.106
1.237
1.349
1.415
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
C,r Terpineol
Approximate
Level
(ppb)
3
1
2
2
2
1
TABLE B313
Organic Compounds Identified in Base Extract of Sample No.1028
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.535 Diethyl Hexyl Phthalate 3
-------
166
TABLE B314
Volatile Organic Compounds Identified in Sample No. 103S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.074
1.554
1.644
Compound
Chloroform
1,2-Dichloroethane
Dichlorobenzene
Dichloro benzene
Approximate
Level
(ppb)
1
1
1
21
TABLE B315
Organic Compounds Identified in Acid Extract of Sample N0.103A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.423 .
0.888
1.000
1.106
Compound
/
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myrsitate
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
2
1
-------
167
TABLE B316
Organic Compounds Identified in Base Extract of Sample No. 103B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B317
Volatile Organic Compounds Identified in Sample N0.104S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.073
1.477
1.964
2.100
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Acetophenone
Approximate
Level
(ppb)
1
1
1
2
1
-------
168
TABLE B318
Organic Compounds Identified in Acid Extract of Sample N0.104A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time
0.213
0.332
0.405
0.463
0.494
0.567
0.619
0.683
0.777
1.000
1.106
1.348
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
Dichlorobutane
Trichlorobutane
Trichloropentene
Trichlorohexane
Dichloroheptane
Trichlorohexane
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
13
1
4
185
92
31
4
1
3
2
1
TABLE B319
Organic Compounds Identified in Base Extract of Sample No. 104B
Relative
Peak Retention
No. Time
Compound
Approximate
Level
(Ppb)
No peaks over 1 PPB.
-------
169
TABLE B320
Volatile Organic Compounds Identified in Sample No.lOSS
Peak
No.
1
2
. 3
4
5
6
Relative
Retention
Time
1.000
1.076
1.238
1.433
1.514
2.022
Compound
Chloroform
1 ,2-Dichloroethane
Carbon Tetrachloride
Trichloropropane
Trichloroethylene
Tetrachl oroethyl ene
TABLE B321
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.391
0.887
0.945
1.000
1.064
1.104
1.141
1.205
1.229
1.242
1.278
1.352
1.376
1.422
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Pentachloroanisole
Methyl Palmitate
?
Methyl Stearate
?
Co-iH00Oo Methyl Pimarate Isomer
L\ 6L C.
C01H_000 Methyl Pimarate Isomer
L\ 3L L.
Methyl Dihydroabietate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C ^ 22
C1(- Terpineol
Approximate
Level
(ppb)
3
2
2
1
3
22
N0.105A
Approximate
Level
(ppb)
___
3
2
4
1
4
1
1
2
5
5
2
1
2
-------
170
TABLE B322
Organic Compounds Identified in Base Extract of Sample No. 105B
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.843
1.000
1.106
1.285
1.319
1.676
2.040
2.498
Compound
?
Camphor (IS)
?
N,N-Di ethyl aniline
Chloroprene Dimer
Di ethyl Phthalate
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
3
3
3
2
1
1
TABLE B323
Volatile Organic Compounds Identified in Sample N0.106S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 5
2 2.007 Tetrachloroethylene 5
3 2.078 C8H]4 1
-------
171
TABLE B324
Organic Compounds Identified in Acid Extract of Sample No.106A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time
0.397
0.550
0.894
0.948
0.985
1.000
1.106
1.139
1.203
1.230
1.252
1.261
1.348
1.370
1.418
1.449
Compound
Methyl -2-Ethyl Hexanoate (IS)
CgH-jg Isomer
Methyl Myri state
Pentachloroanisole
?
Methyl Palmitate
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 20
7
Methyl Dehydroabietate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 22
C-|5 Terpineol
Fatty Acid Methyl Ester C >_ 24
Approximate
Level
(ppb)
_
3
2
2
4
6
6
1
1
1
1
1
2
1
2
1
-------
172
TABLE B325
Organic Compounds Identified in Base Extract of Sample No. 106B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
Relative
Retention
Time
0.531
0.830
1.000
1.107
1.322
1.508
1.571
1.662
1.690
1.769
1.865
2.051
2.086
2.408
2.465
2.521
2.544
2.617
2.645
2.685
2.758
2.837
2.922
2.970
Compound
CfiH-|g Isomer
?
Camphor (IS)
?
Chloroprene Isomer
Hydrocarbon C ^ 16
Dinitrotoluene
?
?
?
?
Di butyl Phthalate
Caffeine
Butyl Phthalyl Butyl Glycolate
Hydrocarbon C >_ 28
Diethyl Hexyl Phthalate
Hydrocarbon C >_ 29
Hydrocarbon C >_ 30
C,5 Terpineol
Hydrocarbon C >_ 31
Hydrocarbon C ^ 32
Hydrocarbon C >_ 33
Hydrocarbon C >_ 34
Hydrocarbon C >_ 35
Approximate
Level
(ppb)
3
1
1
1
2
22
17
20
5
2
1
1
1
1
2
1
1
2
1
1
1
1
1
-------
173
TABLE B326
Volatile Organic Compounds Identified in Sample No. 107S
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.492
1.991
Compound
Chloroform
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
5
1
2
TABLE B327
Organic Compounds Identified in Acid Extract of Sample No.l07A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.414
0.887
1.000
1.107
1.293
1.375
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myristate
Methyl Palmitate
Methyl Stearate
Fatty Acid Methyl Ester C >_ 22
?
Approximate
Level
(ppb)
1
3
4
1
1
-------
174
TABLE B328
Organic Compounds Identified in Base Extract of Sample No.1078
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.484 ? 1
3 2.541 Diethyl Hexyl Phthalate 3
4 2.666 C,5 Terpineol 1
TABLE B329
Volatile Organic Compounds Identified in Sample No.lOSS
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform
2 1.517 Trichloroethylene 2
-------
175
TABLE B330
Organic Compounds Identified in Acid Extract of Sample No. 108A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.439
0.900
1.000
1.121
1.230
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
C,r Terpene
Approximate
Level
(PPb)
2
5
3
2
TABLE B331
Organic Compounds Identified in Base Extract of Sample No. 108B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.740 Diethyl Phthalate 4
3 2.431 Butyl Phthalyl Butyl Glycolate 2
-------
176
TABLE B332
Volatile Organic Compounds Identified in Sample No.1095
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
TABLE B333
Organic Compounds Identified in Acid Extract of Sample N0.109A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.425
1.000
1.104
1.208
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,r Terpene
Approximate
Level
(ppb)
3
2
2
TABLE B334
Organic Compounds Identified in Base Extract of Sample No. 109B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.129 Dibutyl Phthalate 1
3 2.618 Diethyl Hexyl Phthalate 1
-------
177
TABLE B335
Volatile Organic Compounds Identified in Sample No.llOS
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.024
1.317
1.778
Compound
Chloroform
1 ,2-Dichloroethane
Bromo-Dichloromethane
Bromo benzene
Approximate
Level
(ppb)
4
1
2
13
TABLE B336
Organic Compounds Identified in Acid Extract of Sample No.llOA
Peak
No.
1
2
3
4
Relative
Retention
Time
0.400
1.000
1.105
1.350
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_
2
1
1
-------
178
TABLE B337
Organic Compounds Identified in Base Extract of Sample No. HOB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B338
Volatile Organic Compounds Identified in Sample No.lllS
Peak
No.
1
2
3
4
Relative
Retention
Time
0.900
1.000
1.068
1.548
Compound
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
?
Approximate
Level
(ppb)
4
10
2
1
-------
179
TABLE B339
Organic Compounds Identified in Acid Extract of Sample No.lllA
Peak
No.
1
2
3
4
Relative
Retention
Time
0.411
1.000
1.102
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
5
2
2
TABLE B340
Organic Compounds Identified in Base Extract of Sample No. 111B
D L DReJaVVe Approximate
Peak Retention Level
No. Time Compound
1 1.000 Camphor (IS)
2 2.569 Diethyl Hexyl Phthalate 2
3 2.700 C,5 Terpineol 2
4 2.837 ? 1
5 3.001 ? 1
-------
180
TABLE B341
Volatile Organic Compounds Identified in Sample No. 112S
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.074
1.400
1.801
1.896
2.096
Compound
Chloroform
1 ,2-Dichloroethane
Trichloropropane
Dichlorobenzene
Dichlorobenzene
Dichlorobenzene
Approximate
Level
(ppb)
3
1
1
12
8
15
TABLE B342
Organic Compounds Identified in Acid Extract of Sample N0.112A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.376
1.000
1.105
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
4
1
1
-------
181
TABLE B343
Organic Compounds Identified in Base Extract of Sample No. 112B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.943 Atrazine 1
3 2.617 Diethyl Hexyl Phthalate 2
TABLE B344
Volatile Organic Compounds Identified in Sample No. 113S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.069 1,2-Dichloroethane 2
3 1.408 Trichloropropane 1
4 1.482 Trichloroethylene 1
5 1.930 Tetrachloroethylene 7
-------
182
TABLE B345
Organic Compounds Identified in Acid Extract of Sample No.1 ISA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.415 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.102 Methyl Stearate 1
TABLE B346
Organic Compounds Identified in Base Extract of Sample No. 113B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.573 Diethyl Hexyl Phthalate 1
-------
183
TABLE B347
Volatile Organic Compounds Identified in Sample N0.114S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.067 1,2-Dichloroethane 1
3 1.392 Trichloropropane 1
4 1.950 Tetrachloroethylene 2
TABLE B348
Organic Compounds Identified in Acid Extract of Sample No.IHA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.426 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate <1
3 1.099 Methyl Stearate 1
-------
184
TABLE B349
Organic Compounds Identified in Base Extract of Sample No. 114B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.045 Dibutyl Phthalate 2
TABLE B350
Volatile Organic Compounds Identified in Sample No. 115S
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.068
1.304
1.403
1.477
1.555
1.964
Compound
Chloroform
1,2-Dichloroethane
Bromo-Dichloromethane
Trichloropropane
Trichloroethylene
Di bromo-Chl oromethane
Tetrachloroethylene
Approximate
Level
(ppb)
87
1
8
1
1
4
1
-------
185
TABLE B351
Organic Compounds Identified in Acid Extract of Sample No.llSA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
TABLE B352
Organic Compounds Identified in Base Extract of Sample No. 115B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.079 Dibutyl Phthalate 1
TABLE B353
Volatile Organic Compounds Identified) in Sample No.llGS
Relative Approximate
Peak Retention Level
No. Time Compound
1 1.000 Chloroform 1
2 1.068 1 ,2-Dichloroethane 1
-------
186
TABLE B354
Organic Compounds Identified in Acid Extract of Sample N0.116A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.425 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.104 Methyl Stearate 1
TABLE B355
Organic Compounds Identified in Base Extract of Sample No.1166
Relative Approximate
Peak Retention Level
No. Time Compound " (ppb)
No peaks over 1 PPB.
TABLE B356
Volatile Organic Compounds Identified in Sample N0.117S
Relative Approximate
Peak Retention Level
No. Time Compound
No peaks over 1 PPB.
-------
187
TABLE B357
Organic Compounds Identified in Acid Extract of Sample No.lUA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.440 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
TABLE B358
Organic Compounds Identified in Base Extract of Sample No. H7B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.614 C15 Terpineol 1
TABLE B359
Volatile Organic Compounds Identified in Sample No. 118S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.627 Bromobenzene 10
-------
188
TABLE B360
Organic Compounds Identified in Acid Extract of Sample No.llSA
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.428
1.000
1.097
1.103
1.344
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Dibutyl Phthalate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
4
1
4
3
TABLE B361
Organic Compounds Identified in Base Extract of Sample No. 118B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
189
TABLE B362
Volatile Organic Compounds Identified in Sample No. 119S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 1.471 Trichloroethylene 1
TABLE B363
Organic Compounds Identified in Acid Extract of Sample No.H9A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.327
0.463
0.553
0.611
0.679
1.000
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloropentane
Trichloropentane
Trichlorohexane
Trichloroheptane
Methyl Palmitate
Approximate
Level
(ppb)
23
12
15
9
2
-------
190
TABLE B364
Organic Compounds Identified in Base Extract of Sample No. 119B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.149 Dibutyl Phthalate 1
TABLE B365
Volatile Organic Compounds Identified in Sample No. 120S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
-------
191
TABLE B366
Organic Compounds Identified in Acid Extract of Sample N0.120A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
TABLE B367
Organic Compounds Identified in Base Extract of Sample No. 120B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B368
Volatile Organic Compounds Identified in Sample No. 121S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform n
-------
192
TABLE B369
Organic Compounds Identified in Acid Extract of Sample N0.121A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
Relative
Retention
Time
0.162
0.281
0.370
0.406
0.449
0.526
0.596
0.666
0.731
0.795
0.859
0.917
0.972
1.000
1.028
1.083
1.132
1.181
1.226
1.272
1.315
Compound
Cg Alcohol
C7 Alcohol
Cg Alcohol
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
CIQ Alcohol
C^ Alcohol
C12 Alcohol
C,3 Alcohol
C,, Alcohol
C,r Alcohol
C]6 Alcohol
C17 Alcohol
Methyl Palmitate
C,g Alcohol
C-,g Alcohol
C2Q Alcohol
C,,., Alcohol
C22 Alcohol
C23 Alcohol
C0/1 Alcohol
Approximate
Level
(ppb)
2
2
6
8
15
10
8
8
9
5
4
2
1
2
2
2
2
2
2
1
-------
193
TABLE B370
Organic Compounds Identified in Base Extract of Sample No. 121B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B371
Volatile Organic Compounds Identified in Sample No. 122S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform i
TABLE B372
Organic Compounds Identified in Acid Extract of Sample N0.122A
Relative Approximate
Peak Retention Level
No. Time Compound (PPb)
1 0.414 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
-------
194
TABLE B373
Organic Compounds Identified in Base Extract of Sample No. 122B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B374
Volatile Organic Compounds Identified in Sample No. 123S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
TABLE B375
Organic Compounds Identified in Acid Extract of Sample N0.123A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.449 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.102 Methyl Stearate 1
-------
195
TABLE B376
Organic Compounds Identified in Base Extract of Sample No. 123B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B377
Volatile Organic Compounds Identified in Sample No. 124S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
-------
196
TABLE B378
Organic Compounds Identified in Acid Extract of Sample N0.124A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.401
0.897
1.000
1.018
1.067
1.109
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
C,Q Terpineol
?
Methyl Stearate
Approximate
Level
(ppb)
___
1
3
2
2
4
TABLE B379
Organic Compounds Identified in Base Extract of Sample No. 124B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.565 Diethyl Hexyl Phthalate 3
-------
197
TABLE B380
Volatile Organic Compounds Identified in Sample No. 125S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform n
TABLE B381
Organic Compounds Identified in Acid Extract of Sample N0.125A
Peak
No.
1
2
3
Relative
Retention
Time
0.423
1.000
1.100
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
2
2
-------
198
TABLE B382
Organic Compounds Identified in Base Extract of Sample No. 125B
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.914
2.088
2.452
Compound
Camphor (IS)
Atrazine
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Approximate
Level
(ppb)
___
1
2
1
TABLE B383
Volatile Organic Compounds Identified in Sample No. 126S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 2.298 Bromobenzene 5
-------
199
TABLE B384
Organic Compounds Identified in Acid Extract of Sample No.l26A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.433 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
TABLE B385
Organic Compounds Identified in Base Extract of Sample No. 126B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B386
Volatile Organic Compounds Identified in Sample No. 127S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
-------
200
TABLE B387
Organic Compounds Identified in Acid Extract of Sample N0.127A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 4
3 1.111 Methyl Stearate 5
TABLE B388
Organic Compounds Identified in Base Extract of Sample No. 127B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.942 Atrazine 1
-------
201
TABLE B389
Volatile Organic Compounds Identified in Sample No. 128S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.357
1.633
2.232
Compound
Chloroform
Bromo-Dichloroethane
Di bromo-Chl oromethane
Dichloro benzene
^s"
Approximate
Level
(ppb)
40
10
8
10
TABLE B390
Organic Compounds Identified in Acid Extract of Sample N0.128A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B391
Organic Compounds Identified in Base Extract of Sample No. 128B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
202
TABLE B392
Volatile Organic Compounds Identified in Sample No. 129S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
TABLE B393
Organic Compounds Identified in Acid Extract of Sample No. 129A
Relative Approximate
Peak Retention Level
No. Time Compound (PPb)
No peaks over 1 PPB.
TABLE.B394
Organic Compounds Identified in Base Extract of Sample No. 129B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.058 Dibutyl Phthalate 2
-------
203
TABLE B395
Volatile Organic Compounds Identified in Sample No. 130S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 18
2 2.159 Acetophenone 2
TABLE B396
Organic Compounds Identified in Acid Extract of Sample No. 130A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.431
1.000
1.104
1.208
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
Approximate
Level
(ppb)
_
2
1
1
-------
204
TABLE B397
Organic Compounds Identified in Base Extract of Sample No. 130B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B398
Volatile Organic Compounds Identified in Sample No. 131S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.448 Dimethyl Disulfide 1
-------
205
TABLE B399
Organic Compounds Identified in Acid Extract of Sample No.lSIA
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.410
1.000
1.092
1.101
1.275
Compound
Methyl -2- Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
4
1
4
7
TABLE B400
Organic Compounds Identified in Base Extract of Sample No. 131B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.906 Atrazine 1
3 2.028 ? 1
4 2.074 Dibutyl Phthalate 1
5 2.682 Diethyl Hexyl Phthalate 1
-------
206
TABLE B401
Volatile Organic Compounds Identified in Sample No. 132S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 15
2 2.076 Toluene 3
TABLE B402
Organic Compounds Identified in Acid Extract of Sample N0.132A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.424
1 . 000 .
1.031
1.101
1.132
1.350
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
C18 Alcohol
Methyl Stearate
Cp0 Alcohol
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
5
1
5
1
1
-------
207
TABLE B403
Organic Compounds Identified in Base Extract of Sample No.1326
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.994
2.129
2.185
2.682
2.817
Compound
Camphor (IS)
Atrazine
?
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,5 Terpineol
Approximate
Level
(ppb)
1
1
1
1
1
TABLE B404
Volatile Organic Compounds Identified in Sample No. 133S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.273 Cyclohexane 1
3 1.506 Dimethyl Disulfide 1
-------
208
TABLE B405
Organic Compounds Identified in Acid Extract of Sample N0.133A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.431 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Pa Imitate 2
3 1.104 Methyl Stearate 3
TABLE B406
Organic Compounds Identified in Base Extract of Sample No. 133B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.104 Dibutyl Phthalate 1
3 2.575 Diethyl Hexyl Phthalate 1
4 2.708 C15 Terpineol 1
-------
209
TABLE B407
Volatile Organic Compounds Identified in Sample No. 134S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B408
Organic Compounds Identified in Acid Extract of Sample N0.134A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.430
0.908
1.000
1.089
1.110
1.126
1.218
1.288
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
C,,- Terpene
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
Approximate
Level
(ppb)
2
5
4
4
3
2
3
-------
210
TABLE B409
Organic Compounds Identified in Base Extract of Sample No. 134B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.117 Dibutyl Phthalate 1
3 2.590 Diethyl Hexyl Phthalate 1
4 2.725 C]5 Terpineol 1
TABLE B410
Volatile Organic Compounds Identified in Sample No. 135S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.071 1,2-Dichloroethane 2
3 1.547 Benzene 3
-------
211
TABLE B411
Organic Compounds Identified in Acid Extract of Sample No. 135A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.391 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.107 Methyl Stearate 1
4 1.359 Diethyl Hexyl Phthalate 1
TABLE B412
Organic Compounds Identified in Base Extract of Sample No. 135B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.576 C,Q Terpineol 1
3 2.606 Diethyl Hexyl Phthalate 1
-------
212
TABLE B413
Volatile Organic Compounds Identified in Sample No. 136S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.071 1,2-Dichloroethane 3
3 1.296 Dichlorobenzene 1
TABLE B414
Organic Compounds Identified in Acid Extract of Sample No. 136A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.373
0.814
1.000
1.100
1.343
Compound
Methyl -2-Ethyl Hexanoate (IS)
C.Q Terpineol
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
1
6
3
4
-------
213
TABLE B415
Organic Compounds Identified in Base Extract of Sample No.1366
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.516 C]0 Terpineol 1
TABLE B416
Volatile Organic Compounds Identified in Sample No. 137S
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.490
1.630
Compound
Chloroform
Benzene
Hexane
Approximate
Level
(ppb)
1
2
2
-------
214
TABLE B417
Organic Compounds Identified in Acid Extract of Sample No. 137A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.379
0.818
0.912
1.000
1.100
1.118
1.205
1.341
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
C,Q Terpineol
Methyl Palmitate
Methyl Stearate
C,5 Terpene
C,,- Terpene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
2
5
2
1
1
1
TABLE B418
Organic Compounds Identified in Base Extract of Sample No. 137B
Relative Approximate
Peak Retention Level
No. Time Compound (PPb)
1 1.000 Camphor (IS)
2 2.500 Diethyl Hexyl Phthalate 1
-------
215
TABLE B419
Volatile Organic Compounds Identified in Sample No. 138S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.501 Benzene 1
3 1.636 Hexane 1
TABLE B420
Organic Compounds Identified in Acid Extract of Sample No. 138A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.380
0.823
0.891
0.947
1.000
1.094
1.332
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpinebl
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Pa Imitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_
1
3
1
13
6
2
-------
216
TABLE B421
Organic Compounds Identified in Base Extract of Sample No. 138B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.495 Diethyl Hexyl Phthalate 4
TABLE B422
Volatile Organic Compounds Identified in Sample No. 139S
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.467
0.817
1.000
1.302
1.479
1.555
Compound
Acetone
Pentene
Chloroform
Bromo-Di chl oromethane
Trichloroethylene
Di bromo-Chl oromethane
Approximate
Level
(ppb)
1
1
40
7
5
7
-------
217
TABLE B423
Organic Compounds Identified in Acid Extract of Sample No. I39A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.380
1.000
1.102
1.341
1.407
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
C,,- Terpineol
Approximate
Level
(ppb)
_
2
1
1
4
TABLE B424
Organic Compounds Identified in Base Extract of Sample No. 139B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
218
TABLE B425
Volatile Organic Compounds Identified in Sample No. 140S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.302
1.490
2.077
Compound
Chloroform
Chloroprene
Trichloroethylene
Toluene
Approximate
Level
(ppb)
1
1
1
2
TABLE B426
Organic Compounds Identified in Acid Extract of Sample No. 140A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.193
0.401
1.000
1.101
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
3
5
-------
219
TABLE B427
Organic Compounds Identified in Base Extract of Sample No.1408
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B428
Volatile Organic Compounds Identified in Sample No. 141S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.386
1.000
1.219
1.493
2.084
Compound
Dichloromethane
Chloroform
Carbon Tetrachloride
Trichloroethylene
Toluene
Approximate
Level
(ppb)
1
1
1
1
1
-------
220
TABLE B429
Organic Compounds Identified in Acid Extract of Sample No. 141A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.390 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.099 Methyl Stearate 3
4 1.338 Diethyl Hexyl Phthalate 1
TABLE B430
Organic Compounds Identified in Base Extract of Sample No. 141B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.570 Diethyl Hexyl Phthalate 1
-------
221
TABLE B431
Volatile Organic Compounds Identified in Sample No. 142S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.357
0.423
1.000
1.061
.1.091
1.187
1.258
1.400
1.409
1.476
1.931
Compound
Dichloromethane
Acetone
Chloroform
1 ,2-Dichloroethane
Methacrylonitrile
Carbon Tetrachloride
Bromo-Di chl oromethane
Trichloroethylene
Benzene
Bromo-Trichloropropane
Toluene
TABLE B432
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
3
4
Relative
Retention
Time
0.390
1.000
1.098
1.337
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
3
3
1
1
2
1
1
1
2
1
of Sample No. 142A
Approximate
Level
(ppb)
2
1
3
-------
222
TABLE B433
Organic Compounds Identified in Base Extract of Sample No. 142B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.115 Diethyl Hexyl Phthalate 2
TABLE B434
Volatile Organic Compounds Identified in Sample No. 143S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1. PPB.
-------
223
TABLE B435
Organic Compounds Identified in Acid Extract of Sample No. 143A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.419 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.102 Methyl Stearate 1
TABLE B436
Organic Compounds Identified in Base Extract of Sample No. 143B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.057 Dibutyl Phthalate 1
I TABLE B437
Volatile Organic Compounds Identified in Sample No. 144S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
-------
224
TABLE B438
Organic Compounds Identified in Acid Extract of Sample No. 144A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.339 Diethyl Hexyl Phthalate 1
TABLE B439
Organic Compounds Identified in Base Extract of Sample No.l44B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B440
Volatile Organic Compounds Identified in Sample No. 145S
Peak
No.
1
2
3
4
Relative
Retention
Time
1 . 000
1.236
1.330
1.599
Compound
Chloroform
Carbon Tetrachloride
Bromo-Dichloromethane
Dibromo-Chloromethane
Approximate
Level
(ppb)
43
3
7
5
-------
225
TABLE B441
Organic Compounds Identified in Acid Extract of Sample No. 145A
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.326
0.492
1.000
1.091
1.238
1.335
1.354
1.372
1.381
1.406
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Dioctyl Adi pate
Diethyl Hexyl Phthalate Isomers
Diethyl Hexyl Phthalate Isomers
Diethyl Hexyl Phthalate Isomers
Diethyl Hexyl Phthalate Isomers
C15 Terpineol
Approximate
Level
(ppb)
1
4
4
86
4
6
17
26
1
TABLE B442
Organic Compounds Identified in Base Extract of Sample No. 145B
Relative
Peak Retention
No. Time
Compound
Approximate
Level
(ppb)
No peaks over 1 PPB.
-------
226
TABLE B443
Volatile Organic Compounds Identified in Sample No. 146S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.279 Bromo-Dichloromethane 1
TABLE B444
Organic Compounds Identified in Acid Extract of Sample No. 146A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.271
0.412
1.000
1.088
1.099
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Approximate
Level
(ppb)
1
5
1
2
-------
227
TABLE B445
Organic Compounds Identified in Base Extract of Sample No. 146B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 No peaks over 1 PPB.
TABLE B446
Volatile Organic Compounds Identified in Sample No.147S
Peak
No.
1
2
3
4
Relative
Retention
Time
0.422
1.000
1.319
1.583
Compound
Acetone
Chloroform
Bromo-Di chl oromethane
Dibromo-chloromethane
Approximate
Level
(ppb)
1
38
14
4
-------
228
TABLE B447
Organic Compounds Identified in Acid Extract of Sample No. 147A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.410
1.000
1.089
1.100
1.236
1.340
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Dioctyl Adi pate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
5
1
3
4
1
TABLE B448
Organic Compounds Identified in Base Extract of Sample No. 147B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS) .
2 2.011 Dibutyl Phthalate 1
3 2.461 Diethyl Hexyl Phthalate 1
-------
229
TABLE B449
Volatile Organic Compounds Identified in Sample No. 148S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.359 Bromo-Dichloromethane 3
TABLE B450
Organic Compounds Identified in Acid Extract of Sample No. 148A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.341 1,1 ,2,2-Tetrachloroethane 2
2 0.430 Methyl-2-Ethyl Hexanoate (IS)
TABLE B451
Organic Compounds Identified in Base Extract of Sample No. I486
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.011 Dibutyl Phthalate 1
-------
230
TABLE B452
Volatile Organic Compounds Identified in Sample No.149S
Relative Approximate
Peak Retention . Level
No. Time Compound (ppb)
1 1.000 Chloroform 6
2 1.500 Benzene 2
TABLE B453
Organic Compounds Identified in Acid Extract of Sample No. 149A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.418
1.000
1.009
1.100
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
C,r Terpene
Methyl Stearate
Approximate
Level
(ppb)
2
1
2
TABLE B454
Organic Compounds Identified in Base Extract of Sample No. 149B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
231
TABLE B455
Volatile Organic Compounds Identified in Sample No. 150S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.402 Dichloromethane 2
2 1.000 Chloroform 2
TABLE B456
Organic Compounds Identified in Acid Extract of Sample No. 150A
Peak
No.
1
2
3
Relative
Retention
Time
0.410
1.000
1.108
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
1
TABLE B457
Organic Compounds Identified in Base Extract of Sample No. 150B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
232
TABLE B458
Volatile Organic Compounds Identified in Sample No. 151S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B459
Organic Compounds Identified in Acid Extract of Sample No. 151A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.410
0.850
0.955
1.000
1.102
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
?
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
~ -. -»
102
64
11
4
TABLE B460
Organic Compounds Identified in Base Extract of Sample No. 151B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.449 Diethyl Hexyl Phthalate 1
-------
233
TABLE B461
Volatile Organic Compounds Identified in Sample No. 152S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B462
Organic Compounds Identified in Acid Extract of Sample No. 152A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.419
1.000
1.098
1.329
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
.
6
3
2
TABLE B463
Organic Compounds Identified in Base Extract of Sample No. 152B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.009 Dibutyl Phthalate 1
-------
234
TABLE B464
Volatile Organic Compounds Identified in Sample No. 153S
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.335
1.588
Compound
Chloroform
Bromo-Dichloromethane
Dibromo-Chloromethane
Approximate
Level
(ppb)
24
4
4
TABLE B465
Organic Compounds Identified in Acid Extract of Sample No. 153A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.362
0.435
0.471
0.543
0.610
0.676
0.740
0.800
0.861
0.921
0.976
Compound
Cg Alcohol
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
C,Q Alcohol
C^ Alcohol
C]2 Alcohol
C13 Alcohol
C14 Alcohol
C-|5 Alcohol
C,c Alcohol
1 D
C,-, Alcohol
Approximate
Level
(ppb)
2
7
8
9
7
6
8
5
4
1
-------
235
TABLE B466
Organic Compounds Identified in Base Extract of Sample No.1538
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B467
Volatile Organic Compounds Identified in Sample No. 154S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B468
Organic Compounds Identified in Acid Extract of Sample No. 154A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
236
TABLE B469
Organic Compounds Identified in Base Extract of Sample No. 154B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2. 2.043 Diethyl Hexyl Phthalate 2
TABLE B470
Volatile Organic Compounds Identified in Sample No. 155S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B471
Organic Compounds Identified in Acid Extract of Sample No. 155A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.412
1.000
1.105
1.187
1.146
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Unidentified Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
2
3
. 4
-------
237
TABLE B472
Organic Compounds Identified in Base Extract of Sample No.l55B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B473
Volatile Organic Compounds Identified in Sample No. 156S
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.330
1.588
<
Compound
Chloroform
Bromo-Dichloromethane
Di bromo-Chl oromethane
Approximate
Level
(ppb)
29
2
2
TABLE B474
Organic Compounds Identified in Acid Extract of Sample N0.156A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.420 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.107 Methyl Stearate 2
-------
238
TABLE B475
Organic Compounds Identified in Base Extract of Sample No. 156B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.023 Dibutyl Phthalate 2
3 2.470 Diethyl Hexyl Phthalate 1
TABLE B476
Volatile Organic Compounds Identified in Sample No. 157S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.500 Trichloroethylene 1
-------
239
TABLE B477
Organic Compounds Identified in Acid Extract of Sample No. 157A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.434
0.910
1.000
1.102
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,r Terpene
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
_ _
1
3
3
TABLE B478
Organic Compounds Identified in Base Extract of Sample No.l57B
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
1.000
2.023
2.415
2.470
2.559
2.597
2.631
2.696
2.774
2.857
Compound
Camphor (IS)
Dibutyl Phthalate
Hydrocarbon C
Di ethyl Hexyl
Hydrocarbon C
C,g Terpineol
Hydrocarbon C
Hydrocarbon C
Hydrocarbon C
Hydrocarbon C
1 24
Phthalate
I26
1 28
> 28
>_ 30
>_ 30
Approximate
Level
(ppb)
5
1
2
1
2
1
1
1
1
-------
240
TABLE B479
Volatile Organic Compounds Identified in Sample No. 158S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1-000 Chloroform c
TABLE B480
Organic Compounds Identified in Acid Extract of Sample No. 158A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.420
0.896
1.000
1.107
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
___
6
16
2
TABLE B481
Organic Compounds Identified in Base Extract of Sample N0.158B
Relative Approximate
Peak Retention Level
No. Time Compound
No peaks over 1 PPB.
-------
241
TABLE B482
Volatile Organic Compounds Identified in Sample No. 159S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B483
Organic Compounds Identified in Acid Extract of Sample No. 159A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.420 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 6
3 1.103 Methyl Stearate 4
TABLE B484
Organic Compounds Identified in Base Extract of Sample No. 159B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
242
TABLE B485
Volatile Organic Compounds Identified in Sample No. 160S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 7
TABLE B486
Organic Compounds Identified in Acid Extract of Sample No. 160A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B487
Organic Compounds Identified in Base Extract of Sample No. 160B
Relative . Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
243
TABLE B488
Volatile Organic Compounds Identified in Sample No. 161S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B489
Organic Compounds Identified in Acid Extract of Sample No. 161A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B490
Organic Compounds Identified in Base Extract of Sample No. 161B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
244
TABLE B491
Volatile Organic Compounds Identified in Sample No. 162S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
TABLE B492
Organic Compounds Identified in Acid Extract of Sample No. 162A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B493
Organic Compounds Identified in Base Extract of Sample No.l62B
Relative Approximate
Peak Retention Level
No. Time Compound (PPb)
No peaks over 1 PPB.
-------
245
TABLE B494
Volatile Organic Compounds Identified in Sample No. 163S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B495
Organic Compounds Identified in Acid Extract of Sample No. 163A
Peak
No.
1
2
3
Relative
Retention
Time
0.321
0.420
1.000
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Approximate
Level
(ppb)
1
2
TABLE B496
Organic Compounds Identified in Base Extract of Sample No.1638
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.496 Diethyl Hexyl Phthalate 1
-------
246
TABLE B497
Volatile Organic Compounds Identified in Sample No. 164S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B498
Organic Compounds Identified in Acid Extract of Sample No.l64A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B499
Organic Compounds Identified in Base Extract of Sample No. 164B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.983 Diisobutyl Phthalate 4
3 2.092 Dibutyl Phthalate 7
-------
247
TABLE B500
Volatile Organic Compounds Identified in Sample No. 165S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.846 Tetrahydrofuran 3
2 1.000 Chloroform 4
3 1.618 Hexanol 2
TABLE B501
Organic Compounds Identified in Acid Extract of Sample No. 165A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B502
Organic Compounds Identified in Base Extract of Sample No. 165B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
248
TABLE B503
Volatile Organic Compounds Identified in Sample No. 166S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B504
Organic Compounds Identified in Acid Extract of Sample No. 166A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B505
Organic Compounds Identified in Base Extract of Sample No. 166B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
249
TABLE B506
Volatile Organic Compounds Identified in Sample No. 167S
Peak
No.
1
2
Relative
Retention
Time
0.390
1.465
Compound
Dichloromethane
Benzene
Approximate
Level
(ppb)
5
1
TABLE B507
Organic Compounds Identified in Acid Extract of Sample No. 167A
Peak
No.
1
2
3
Relative
Retention
Time
0.387
1.000
1.288
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Butyl Phthalyl Butyl Glycolate
Approximate
Level
(ppb)
2
2
TABLE B508
Organic Compounds Identified in Base Extract of Sample No. 167B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
250
TABUE B509
Volatile Organic Compounds Identified in Sample No. 168S
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.879
0.949
1.000
1.440
1 . 546
1.919
2.026
Compound
Tetrahydrofuran
1 ,2-Dichloroethane
Chloroform
Trichloroethylene
Methyl -t-Butyl Ketone
Tetrachl oroethyl ene
Dichlorobenzene
TABLE B510
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.349
0.434
0.568
0.678
0.705
0.781
0.933
0.969
1.000
1.103
1.140
1.255
1.346
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Pentachlorobutene
CxHyClz, x ^4, z i 5
CxHyC1z' x ^4, z i 5
Pentachloroethane
Hexachlorobenzene
?
Methyl Palmitate
Methyl Stearate
?
?
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
318
4
9
188
1
45
2
of Sample N0.168A
Approximate
Level
(ppb)
1
1
6
7
1
3
2
3
2
1
3
1
-------
251
TABLE B511
Organic Compounds Identified in Base Extract of Sample No. 168B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
Relative
Retention
Time
0.580
0.762
0.784
0.817
0.878
0.917
0.934
0.955
0.972
1.000
1.016
1.083
1.127
1.182
1.221
1.271
1.359
1.387
1.409
1.448
1.503
1.691
2.420
Compound
Tetrachloroe thane
Hexachloroethane
Tetrachlorobutadiene
Tetrachl orobutadi ene
Pentachlorobutadiene
Tetrachlorobutadiene
Pentachlorobutadiene
Pentachlorobutadiene
He xachl orobutadi ene
Camphor (IS)
Pentachlorobutene
Pentachlorobutene
Hexachlorobutene
Hexachlorobutene
C H Cl , x > 4, z > 5
x y z
CH Cl . x > 4, z > 5
x y z
C H Cl . x > 4, z > 5
x y z
C H Cl , x > 4, z > 5
x y z
C H Cl , x > 4, z > 5
x y z - -
Pentachloroethane
Pentachloroe thane
Hexachlorobenzene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
44
3
5
7
6
11
5
38
22
64
27
21
17
99
100
14
3
13
1
2
4
2
-------
252
TABLE B512
Volatile Organic Compounds Identified in Sample No. 169S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.877 Tetrahydrofuran 2
TABLE B513
Organic Compounds Identified in Acid Extract of Sample No. 169A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.352
0.431
1.000
1.021
1.104
1.239
1.376
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
?
?
?
Approximate
Level
(ppb)
1
5
1
2
4
1
-------
253
TABLE B514
Organic Compounds Identified in Base Extract of Sample No.l69B
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.147
1.413
Compound
Camphor (IS)
2-Methyl Thiobenzothiazole
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
3
1
TABLE B515
Volatile Organic Compounds Identified in Sample No.170S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B516
Organic Compounds Identified in Acid Extract of Sample No. 170A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.410
1.000
1.065
1.108
1.244
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Approximate
Level
(ppb)
3
1
3
3
-------
254
TABLE B517
Organic Compounds Identified in Base Extract of Sample No. 170B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.081 Dibutyl Phthalate 1
3 2.561 Diethyl Hexyl Phthalate 1
TABLE B518
Volatile Organic Compounds Identified in Sample No. 171S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
255
TABLE B519
Organic Compounds Identified in Acid Extract of Sample No. 171A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
Relative
Retention
Time
0.306
0.324
0.420
0.420
0.468
0.543
0.612
0.678
0.742
0.805
0.865
0.892
0.922
0.979
1.000
1.033
1.084
1.102
1.129
1.180
1.222
1.267
1.309
1.348
1.387
1.414
Compound
C7 Alcohol
Dichlorobutene
Cg Alcohol
Methyl -2- Ethyl Hexanoate (IS)
Cg Alcohol
C-JQ Alcohol
C^ Alcohol
C]2 Alcohol
C13 Alcohol
C,. Alcohol
C15 Alcohol
Methyl Myri state
C]6 Alcohol
C17 Alcohol
Methyl Palmitate
C18 Alcohol
C,g Alcohol
Methyl Stearate
C2Q Alcohol
C21 Alcohol
C22 Alcohol
C23 Alcohol
C24 Alcohol
Diethyl Hexyl Phthalate +
C25 Alcohol
C26 Alcohol
C Terpineol
Approximate
Level
(ppb)
1
1
1
2
2
2
3
3
3
3
1
3
4
12
6
4
16
7
5
6
4
3
3
2
1
-------
256
TABLE B520
Organic Compounds Identified in Base Extract of Sample No.l71B
Peak
No.
1
2
3
Relative
Retention
Time
1.000
2.019
2.500
Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _
1
1
TABLE B521
Volatile Organic Compounds Identified in Sample No. 172S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B522
Organic Compounds Identified in Acid Extract of Sample No. 172A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.342
0.421
1.000
1.107
1.355
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
6
8
6
-------
257
TABLE B523
Organic Compounds Identified in Base Extract of Sample No. 172B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B524
Volatile Organic Compounds Identified in Sample No. 173S
Peak
No.
1
Relative
Retention
Time
1.000
Compound
Chloroform
Approximate
Level
(ppb)
4
TABLE B525
Organic Compounds Identified in Acid Extract of Sample No. 173A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.411 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.107 Methyl Stearate 1
-------
258
TABLE B526
Organic Compounds Identified in Base Extract of Sample No.1736
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.001 Dibutyl Phthalate 2
TABLE B527
Volatile Organic Compounds Identified in Sample No. 174S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
TABLE B528
Organic Compounds Identified in Acid Extract of Sample No. 174A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
259
TABLE B529
Organic Compounds Identified in Base Extract of Sample No. 174B
Relative Approximate
Peak Retention Level
No. Time Compound " (ppb)
No peaks over 1 PPB.
TABLE B530
Volatile Organic Compounds Identified in Sample No.l75S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B531
Organic Compounds Identified in Acid Extract of Sample No. USA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.427 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl PaImitate 1
3 1.104 Methyl Stearate 1
-------
260
TABLE B532
Organic Compounds Identified in Base Extract of Sample No.1756
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B533
Volatile Organic Compounds Identified in Sample No.176S
Peak
No.
1
2
3
4
Relative
Retention
Time
0.397
0.673
1.000
1.459
Compound
Dimethyl Sulfide
Di me thoxyme thane
Chloroform
Dimethyl Disulfide
Approximate
Level
(ppb)
1
3
1
1
TABLE B534
Organic Compounds Identified in Acid Extract of Sample No.l76A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Methyl Palmitate 6
2 1.104 Methyl Stearate 3
3 1.120 C ~ TerPene 1
-------
261
TABLE B535
Organic Compounds Identified in Base Extract of Sample No.1768
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.082 Dibutyl Phthalate 1
3 2.563 Diethyl Hexyl Phthalate 1
TABLE B536
Volatile Organic Compounds Identified in Sample No. 177S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
262
TABLE B537
Organic Compounds Identified in Acid Extract of Sample No. 177A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.426
0.475
0.543
0.607
0.678
0.739
0.801
0.862
0.920
0.975
1.031
Compound
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
C,Q Alcohol
C,, Alcohol
C,2 Alcohol
C,3 Alcohol
C,. Alcohol
C-|5 Alcohol
C16 Alcohol
C,7 Alcohol
C-jg Alcohol
Approximate
Level
(ppb)
1
1
1
4
3
3
2
2
1
1
TABLE B538
Organic Compounds Identified in Base Extract of Sample No. 177B
Relative
Peak Retention
No. Time
Compound
Approximate
Level
(ppb)
1 1.000
2 2.589
Camphor
Diethyl Hexyl Phthalate
-------
263
TABLE B539
Volatile Organic Compounds Identified in Sample No. 178S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
TABLE B540
Organic Compounds Identified in Acid Extract of Sample N0.178A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.522
0.595
0.667
0.731
0.796
0.858
Compound
C,Q Alcohol
C,, Alcohol
C,2 Alcohol
C13 Alcohol
C,. Alcohol
C,,- Alcohol
1 b
Approximate
Level
(ppb)
2
3
2
3
3
2
-------
264
TABLE B541
Organic Compounds Identified in Base Extract of Sample No.1788
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.578 Diethyl Hexyl Phthalate 1
TABLE B542
Volatile Organic Compounds Identified in Sample N0.179S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 8
TABLE B543
Organic Compounds Identified in Acid Extract of Sample No. 179A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.408 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.105 Methyl Stearate 1
-------
265
TABLE B544
Organic Compounds Identified in Base Extract of Sample No.l79B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.606 Dichlorobutane 5
2 1.000 Camphor (IS)
TABLE B545
Volatile Organic Compounds Identified in Sample No. 180S
Relative Approximate
Peak Retention Level
No. Time Compound . (ppb)
1 1.000 Chloroform 2
2 1.065 1,2-Dichloroethane 1
-------
266
TABLE B546
Organic Compounds Identified in Acid Extract of Sample No.lSOA
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Relative
Retention
Time
0.426
0.742
0.804
0.862
0.920
0.978
1.000
1.031
1.086
1.108
1.135
1.181
1.227
1.273
1.353
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,- Alcohol
C]4 Alcohol
C,5 Alcohol
C,c Alcohol
ID
C,7 Alcohol
Methyl Palmitate
C,0 Alcohol
its
C,g Alcohol
Methyl Stearate
C2Q Alcohol
C01 Alcohol
21
C22 Alcohol
C23 Alcohol
Diethyl Hexyl Phthalate
TABLE B547
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
Relative
Retention
Time
0.645
1.000
2.532
Compound
Dichlorobutane
Camphor (IS)
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
2
2
2
2
4
1
1
3
1
1
1
1
2
No. 1 SOB
Approximate
Level
(ppb)
3
1
-------
267
TABLE B548
Volatile Organic Compounds Identified in Sample No. 181S
Peak
No.
1
2
Relative
Retention
Time
1.000
1.177
Compound
Chloroform
1 ,1 ,1-Trichloroethane
Approximate
Level
(ppb)
3
1
TABLE B549
Organic Compounds Identified in Acid Extract of Sample No. 181A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.481
0.904
1.000
1.120
1.278
1.352
1.447
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,c Terpene
Methyl Palmitate
C,,- Terpene
Methyl Dehydroabietate
?
?
Approximate
Level
(ppb)
_ _ ..
1
3
2
1
1
1
TABLE B550
Organic Compounds Identified in Base Extract of Sample No.lSIB
Relative Approximate
Peak Retention Level
No. Time Compound
1 1.000 Camphor (IS)
2 2.606 Diethyl Hexyl Phthalate
-------
268
TABLE B551
Volatile Organic Compounds Identified in Sample No.1825
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.783 Bromobenzene 3
TABLE B552
Organic Compounds Identified in Acid Extract of Sample No. 182A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.426
1.000
1.089
1.095
1.102
1.230
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Dibutyl Phthalate
Methyl Stearate
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
5
4
3
6
11
2
-------
269
TABLE B553
Organic Compounds Identified in Base Extract of Sample No.1826
Peak
No.
1
2
3
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.627
1.000
2.558
Volatile
Relative
Retention
Time
1.000
1.425
1.725
1.949
2.114
2.421
Compound
Dichlorobutane
Camphor (IS)
Diethyl Hexyl Phthalate
TABLE B554
Organic Compounds Identified in
Compound
Chloroform
1 ,2-Bromo-Chloroe thane
Dibromoethane
Methyl Ethyl Dioxolane
Tetrachl oroethyl ene
Acetophenone
TABLE B555
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
3
4
Relative
Retention
Time
0.379
1.000
1.107
1.352
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
1
Sample No.l83S
Approximate
Level
(ppb)
1
2
4
1
1
1
of Sample No. 183A
Approximate
Level
(ppb)
3
2
1
-------
270
TABLE B556
Organic Compounds Identified in Base Extract of Sample No.1836
Peak
No.
1
2
3
4
Peak
No.
1
2
3
Relative
Retention
Time
0.473
1.000
2.105
2.585
Volatile
Relative
Retention
Time
0.879
1.000
2.146
/
Compound
Dichlorobutane
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
TABLE B557
Organic Compounds Identified in Sample No.
Compound
Tetrahydrofuran
Chloroform
Toluene
TABLE B558
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.305
0.416
1.000
1.108
1.235
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
?
Approximate
Level
(ppb)
4
1
2
184S
Approximate
Level
(ppb)
1
12
1
N0.184A
Approximate
Level
(ppb)
2
2
2
1
-------
271
TABLE B559
Organic Compounds Identified in Base Extract of Sample No. 184B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.689 Diethyl Hexyl Phthalate 1
TABLE B560
Volatile Organic Compounds Identified in Sample No. 185S
Peak
No.
1
2
Relative
Retention
Time
0.948
1.000
Compound
Diethyl Ether
Chloroform
Approximate
Level
(ppb)
4
11
TABLE B561
Organic Compounds Identified in Acid Extract of Sample N0.185A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.420
1.000
1.065
1.116
1.174
1.371
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
...
1
13
1
2
1
-------
272
TABLE B562
Organic Compounds Identified in Base Extract of Sample No. 185B
Peak
No.
1
2
3
Relative
Retention
Time
0.542
1.000
2.607
Compound
Dichlorobutane
Camphor (IS)
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
3
1
TABLE B563
Volatile Organic Compounds Identified in Sample No. 186S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B564
Organic Compounds Identified in Acid Extract of Sample N0.186A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.400
1.000
1.103
1.110
1.349
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Dibutyl Phthalate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
1
1
-------
273
TABLE B565
Organic Compounds Identified in Base Extract of Sample No.1866
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.557 Dichlorobutane 9
2 1.000 Camphor (IS)
TABLE B566
Volatile Organic Compounds Identified in Sample No. 187S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 2.239 Toluene 1
TABLE B567
Organic Compounds Identified in Acid Extract of Sample N0.187A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
274
TABLE B568
Organic Compounds Identified in Base Extract of Sample No.1876
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B569
Volatile Organic Compounds Identified in Sample No. 188S
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.157
1.414
1.452
.1.959
2.029
Compound
Chloroform
1 ,1 ,1-Trichloroethane
Dimethyl Disulfide
Trichloroethylene
Tetrachl oroethyl ene
Toluene
Approximate
Level
(ppb)
2
4
1
3
13
2
-------
275
TABLE B570
Organic Compounds Identified in Acid Extract of Sample No.lSSA
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Relative
Retention
Time
0.411
0.487
0.521
0.554
0.591
0.621
0.654
0.688
0.751
0.775
0.806
0.815
0.873
0.887
0.918
0.933
0.945
0.988
1.000
1.021
1.042
1.058
1.073
1.109
1.142
1.160
1.182
1.203
1.212
1.224
1.239
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Hydrocarbon C > 8
Hydrocarbon C > 8
Hydrocarbon C > 10
Hydrocarbon C > 10
Hydrocarbon C > 10
Hydrocarbon C > 10
Hydrocarbon C >_ 12
Hydrocarbon C >_ 12
Hydrocarbon C >_ 12
Tetrachloroanisole
Hydrocarbon C >_ 14
Methyl Myri state
Methyl Naphthoate
Hydrocarbon C >_ 16
Pentachloroanisole
Hydrocarbon C >_ 16
Methyl Palmitate
?
Hydrocarbon C >_ 18
?
?
Methyl Stearate
?
?
Methoxy Carbonyl Benzophenone
?
C16H10
?
?
Approximate
Level
(ppb)
1
1
1
1
1
1
4
6
4
8
10
17
10
3
12
14
1
30
5
17
20
5
87
23
17
27
35
2
37
35
-------
276
TABLE B570, cont.
Organic Compounds Identified in Acid Extract of Sample No.lSSA (continued)
Peak
No.
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
Relative
Retention
Time
1.269
1.279
1.318
1.330
1.351
1.360
1.369
1.388
1.400
1.409
1.418
1.427
1.446
1.457
1.482
1.497
1.536
1.558
1.567
1 . 582
Compound
7
?
?
Fatty Acid Methyl Ester C >_ 20
Di ethyl Hexyl Phthalate
?
Fatty Acid Methyl Ester C >_ 24
?
Hydrocarbon C >_ 28
?
?
?
7
7
7
7
7
7
7
7
Approximate
Level
(ppb)
15
82
18
3
31
80
39
20
10
35
40
31
45
27
42
9
33
10
27
12
-------
277
TABLE B571
Organic Compounds Identified in Base Extract of Sample No.l88B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
Relative
Retention
Time
1.000
1.049
1.146
1.214
1.287
'1.317
1.348
1.378
1.438
1.470
1.531
1.592
1.732
1.787
1.806
2.007
2.032
2.147
2.184
2.221
2.276
2.312
2.349
2.373
2.416
2.440
2.465
2.489
2.550
2.574
Compound
Camphor (IS)
?
?
Hydrocarbon C >_ 12
Methyl Naphthalene
Methyl Naphthalene
Hydrocarbon C >_ 12
Indole
Dimethyl Naphthalene
Dimethyl Naphthalene
?
Biphenyl
Methyl Acenaphthene
Diethyl Phthalate
7
Phenanthrene
Diisobutyl Phthalate
?
Dibutyl Phthalate
Caffeine
Hydrocarbon. C >_ 20
Hydrocarbon C >_ 20
C16H10
Hydrocarbon C ^ 22
C16H10
Hydrocarbon C ^ 22
Hydrocarbon C >_ 22
Hydrocarbon C >_ 22
Hydrocarbon C >_ 24
Hydrocarbon C >_ 24
Approximate
Level
(ppb)
3
2
1
1
1
3
11
3
3
3
2
2
2
1
1
2
4
8
6
5
1
1
1
1
1
1
1
2
1
-------
278
TABLE B571, cont.
Organic Compounds Identified in Base Extract of Sample No.1886 (continued)
Peak
No.
31
32
33
34
35
36
37
38
39
Relative
Retention
Time
2.636
2.691
2.709
2.752
2.825
2.910
2.989
3.069
3.173
Compound
Hydrocarbon C > 24
Diethyl Hexyl Phthalate
Hydrocarbon C >_ 26
Hydrocarbon C ^ 26
C,,- Terpineol
?
?
?
?
Approximate
Level
(ppb)
2
4
1
1
4
3
3
10
13
TABLE B572
Volatile Organic Compounds Identified in Sample No. 189S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
-------
279
TABLE B573
Organic Compounds Identified in Acid Extract of Sample N0.189A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.342 Diethyl Hexyl Phthalate 1
TABLE B574
Organic Compounds Identified in Base Extract of Sample No.1896
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.692 Diethyl Hexyl Phthalate 1
-------
280
TABLE B575
Volatile Organic Compounds Identified in Sample No.190S
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.412
0.956
1.000
1.544
1.619
1.882
2.194
2.282
Compound
t
Acetone
Diethyl Ether
Chloroform
?
Benzene
Bromobenzene
Tetrachloroethylene
Toluene
TABLE B576
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.356
0.684
0.753
0.798
0.809
0.944
1.000
1.062
1.098
1.104
1.113
1.234
1.278
1.375
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
?
Methyl -2-(4-chlprophenoxy) Butanoate
Tetrachloroanisole
Pentachl oroani sol e
Methyl Palmitate
?
Di butyl Phthalate
Methyl Stearate
Caffeine
?
?
?
Approximate
Level
(ppb)
3
1
3
2
4
8
1
1
N0.190A
Approximate
Level
(ppb)
1
1
2
1
1
2
5
2
5
3
15
. 5
8
-------
281
TABLE B577
Organic Compounds Identified in Base Extract of Sample No.1908
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.856
2.284
2.317
2.389
2.422
2.759
2.837
3.133
Compound
Camphor (IS)
?
Dibutyl Phthalate
Caffeine
Hydrocarbon C >_ 20
?
?
Di ethyl Hexyl Phthalate
?
Approximate
Level
(ppb)
1
2
4
1
1
6
3
1
TABLE B578
Volatile Organic Compounds Identified in Sample No. 191S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.490 Acetone 2
2 1.110 Methyl Ethyl Ketone 23
3 2.274 Benzaldehyde 1
-------
282
TABLE B579
Organic Compounds Identified in Acid Extract of Sample No. 191A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
Relative
Retention
Time
0.400
0.804
0.817
0.872
0.887
0.933
0.948
0.982
1.000
1.033
1.040
1.055
1.064
1.107
1.143
1.159
1.180
1.204
1.216
1.235 .
1.284
1.293
1.353
1.378
1.506
1.595
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl -2- (4-chlorophenoxy) Butanoate
Tetrachloroanisole
Hydrocarbon C > 14
Methyl Myri state
Hydrocarbon C >_ 16
Pentachloroanisole
Fatty Acid Methyl Ester C >_ 15
Methyl Palmitate
?
Fatty Acid Methyl Ester C >_ 16
Fatty Acid Methyl Ester C >_ 17
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 18
Fatty Acid Methyl Ester C >_ 18
?
Fatty Acid Methyl Ester C >_ 20
?
?
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
?
?
7
Approximate
Level
(ppb)
12
14
21
30
33
24
5
252
25
45
49
13
425
34
48
32
70
8
95
40
66
34
57
53
79
-------
283
TABLE B580
Organic Compounds Identified in Base Extract of Sample No.191B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
Relative
Retention
Time
0.549
1.000
1.181
1.310
1.421
1.473
1.532
1.549
1.661
1.729
1.755
1.748
1.819
1.877
2.029
2.088
2.182
2.217
2.270
2.339
2.469
2.515
2.586
2.703
Compound
Dichlorobutane
Camphor (IS)
Hydrocarbon C > 10
Hydrocarbon C > 12
Hydrocarbon C > 12
Hydrocarbon C > 12
Hydrocarbon C > 14
Hydrocarbon C > 14
Hydrocarbon C > 14
?
Hydrocarbon C > 16
Hydrocarbon C >_ 16
Hydrocarbon C > 16
Hydrocarbon C > 16
Hydrocarbon C > 18
Dibutyl Phthalate
Hydrocarbon C 20
Hydrocarbon C 20
?
Hydrocarbon C 22
Hydrocarbon C 24
Hydrocarbon C 24
Diethyl Hexyl Phthalate
C,r Terpineol
Approximate
Level
(ppb)
3
1
1
1
1
3
3
18
13
12
15
20
59
59
60
38
48
123
41
18
20
58
35
-------
284
TABLE B581
Volatile Organic Compounds Identified in Sample No.1925
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
No peaks over 1 PPB.
TABLE B582
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.400
0.602
0.672
0.738
0.801
0.861
0.921
0.979
1.000
1.030 .
1.084
1.099
1.105
1.129
1.181
1.226
1.271
1.287
1.310
1.352
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,, Alcohol
C12 Alcohol
C,3 Alcohol
C,. Alcohol
C15 Alcohol
Cnc Alcohol
1 0
C,7 Alcohol
Methyl Palmitate
CIQ Alcohol
C,g Alcohol
Di butyl Phthalate
Methyl Stearate
C2Q Alcohol
C2-, Alcohol
C22 Alcohol
C23 Alcohol
Butyl Phthalyl Butyl Glycolate
C24 Alcohol
Diethyl Hexyl Phthalate
Sample No. 192A
Approximate
Level
(ppb)
5
7
9
12
15
13
5
5
4
2
2
3
2
2
1
1
1
1
2
-------
285
TABLE B583
Organic Compounds Identified in Base Extract of Sample No. 192B
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.645
1.000
2.076
2.437
2.553
Compound
Dichlorobutane
Camphor (IS)
Di butyl Phthalate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
2
1
3
TABLE B584
Volatile Organic Compounds Identified in Sample N0.193S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
286
TABLE B585
Organic Compounds Identified in Acid Extract of Sample N0.193A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.430
1.000
1.096
1.102
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_
1
1
1
1
TABLE B586
Organic Compounds Identified in Base Extract of Sample No.1936
Peak
No.
1
2
3
4
Relative
Retention
Time
0.570
1.000
2.106
2.595
Compound
Dichlorobutane
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
4
1
1
TABLE B587
Volatile Organic Compounds Identified in Sample No.l94S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
287
TABLE B588
Organic Compounds Identified in Acid Extract of Sample N0.194A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.370
0.442
0.504
0.561
0.623
0.685
0.847
0.807
0.866
0.923
0.979
1.000
1.032
1.083
1.100
1.105
1.130
1.175
1.219
1.343
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
C-JQ Alcohol
C,, Alcohol
C12 Alcohol
C,3 Alcohol
C]4 Alcohol
C,r Alcohol
1 D
C,c Alcohol
1 b
C,7 Alcohol
Methyl Palmitate
C,g Alcohol
C,g Alcohol
Dibutyl Phthalate
Methyl Stearate
C2Q Alcohol
C2, Alcohol
C22 Alcohol
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
3
2
2
3
3
2
1
1
1
2
1
1
1
1
1
1
1
1
-------
288
TABLE B589
Organic Compounds Identified in Base Extract of Sample No.1946
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.789 Diethyl Hexyl Phthalate 2
TABLE B590
Volatile Organic Compounds Identified in Sample No.1955
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
289
TABLE B591
Organic Compounds Identified in Acid Extract of Sample N0.195A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.410
1.000
1.064
1.097
1.107
1.238
1.351
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Dibutyl Phthalate
Methyl Stearate
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
-. _ _
4
2
1
2
2
1
TABLE B592
Organic Compounds Identified in Base Extract of Sample No.l95B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.642 Dichlorobutane 3
2 1.000 Camphor (IS)
3 2.499 Diethyl Hexyl Phthalate 4
-------
290
TABLE B593
Volatile Organic Compounds Identified in Sample No.1965
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B594
Organic Compounds Identified in Acid Extract of Sample N0.196A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.105 Methyl Stearate 1
TABLE B595
Organic Compounds Identified in Base Extract of Sample N0.196B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.666 Dichlorobutane 6
2 1.000 Camphor (IS)
3 2.462 ? 1
-------
291
TABLE B596
Volatile Organic Compounds Identified in Sample N0.197S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B597
Organic Compounds Identified in Acid Extract of Sample N0.197A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.352
0.430
1.000
1.102
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
3
3
TABLE B598
Organic Compounds Identified in Base Extract of Sample No.1978
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.637 Dichlorobutane 7
2 1.000 Camphor (IS)
3 2.451 ? 2
-------
292
TABLE B599
Volatile Organic Compounds Identified in Sample No.1985
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B600
Organic Compounds Identified in Acid Extract of Sample N0.198A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.919
1.976
1.000
1.027
Compound
C,c Alcohol
1 0
C,7 Alcohol
Methyl Palmitate
C-,a Alcohol
Approximate
Level
(ppb)
1
1
1
1
TABLE B601
Organic Compounds Identified in Base Extract of Sample No.1986
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
293
TABLE B602
Volatile Organic Compounds Identified in Sample No.1995
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.502 Butadiene 2
2 1.000 Chloroform 1
TABLE B603
Organic Compounds Identified in Acid Extract of Sample N0.199A
Peak
No.
1
2
3
Relative
Retention
Time
0.420
1.000
1.104
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
___
2
1
TABLE B604
Organic Compounds Identified in Base Extract of Sample No.1996
Peak
No.
1
2
Relative
Retention
Time
0.656
1.000
Compound
Dichlorobutane
Camphor (IS)
Approximate
Level
(ppb)
4
-------
294
TABLE B605
Volatile Organic Compounds Identified in Sample No.200S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B606
Organic Compounds Identified in Acid Extract of Sample No.200A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.280
0.362
0.431
1.000
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Approximate
Level
(ppb)
1
1
1
TABLE B607
Organic Compounds Identified in Base Extract of Sample No. 200B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.653 Dichlorobutane 7
2 1.000 Camphor (IS)
-------
295
TABLE B608
Volatile Organic Compounds Identified in Sample No.201S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B609
Organic Compounds Identified in Acid Extract of Sample N0.201A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.396
0.758
0.804
0.891
1.000
1.103
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
C 14 Alcohol
Methyl Myristate
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
1
2
2
2
-------
296
TABLE B610
Organic Compounds Identified in Base Extract of Sample No.2016
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.659 Dichlorobutane 1
2 1.000 Camphor (IS)
3 2.481 Diethyl Hexyl Phthalate 1
TABLE B611
Volatile Organic Compounds Identified in Sample No.202S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE .8612
Organic Compounds Identified in Acid Extract of Sample No.202A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
297
TABLE B613
Organic Compounds Identified in Base Extract of Sample No.202B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.644 Dichlorobutane 3
2 1.000 Camphor (IS)
TABLE B614
Volatile Organic Compounds Identified in Sample No.203S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
TABLE B615
Organic Compounds Identified in Acid Extract of Sample No.203A
Peak
No.
1
2
3
Relative
Retention
Time
0.443
1.000
1.096
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
1
-------
298
TABLE B616
Organic Compounds Identified in Base Extract of Sample No.2036
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.631 Dichlorobutane 5
2 1.000 Camphor (IS)
3 2.409 Butyl Phthalyl Butyl Glycolate 3
TABLE B617
Volatile Organic Compounds Identified in Sample No.204S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B618
Organic Compounds Identified in Acid Extract of Sample No. 204A
Peak
No.
1
2
3
Relative
Retention
Time
0.420
0.815
1.000
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
Methyl Palmitate
Approximate
Level
(ppb)
_
1
1
-------
299
TABLE B619
Organic Compounds Identified in Base Extract of Sample No.204B
Peak
No.
1
2
3
4
Relative
Retention
Time
0.639
1.000
1.532
2.412
Compound
Dichlorobutane
Camphor (IS)
C,Q Terpineol
?
Approximate
Level
(ppb)
3
3
1
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