MONITORING TO DETECT
PREVIOUSLY UNRECOGNIZED POLLUTANTS
          IN SURFACE  WATERS
                APPENDIX
                JULY 1977
       U.S. ENVIRONMENTAL PROTECTION AGENCY
           OFFICE OF TOXIC SUBSTANCES
            WASHINGTON, D.C. 20460

-------
            77-
                                   TtCHNiCAL REPORT DATA
                               ji1 rcnJ Iinojiictiotis on the reverse before completing)
 \. REPORT NO.

 EPA-560/7-77-001a
 4. TITLE AND SUBTi TLE
 Monitoring to Detect Previously Unrecognized
 Pollutants in Surface Waters—Appendix:  Organic
 Analysis  Data
7. AUTHORtS)
 B. B.  Ewing,  E.S.K.  Chi an, J. C. Cook,  C.  A.  Evans,
 P. K.  Hopke,  E.  G.  Perkins, and J. C. Means	
9. PERFORMING ORGANIZATION NAMF AND ADDRESS
  Institute  for Environmental Studies
 408  S.  Goodwin Avenue
 University of Illinois at Urbana-Champaign
 Urbana,  Illinois  61801
                                                           3. RECIPIENT'S ACCESSION-NO.
                            5. REPORT DATE
                              July 1977
                            6. PERFORMING ORGANIZATION CODE
                                                           8. PERFORMING ORGANIZATION REPORT NO.
                                                           10. PROGRAM ELEMENT NO.
                             11. CONTRACT/GRANT NO.
                              EPA 68-01-3234
 12. SPONSORING AGENCY NAME AND ADDRESS
 United  States  Environmental
 Office  of Toxic Substances
 Washington,  D.  C.   20460
Protection Agency
                                                           13. TYPE OF REPORT AND PERIOD COVERED

                                                            Appendix to  final  report.
14. SPONSORING AGENCY CODE
 15. SUPPLEMENTARY NOTES
 16. ABSTRACT

 Samples  of surface waters were collected  from  204 sites near heavily industrialized
 areas across  the United States.  The samples were analyzed for all contaminants
 present  at concentrations greater than one  part per billion.  Each water  sample
 was  preconcentrated for analysis of organics in three fractions:  volatile
 organics by nitrogen-gas stripping and the  less-volatile organics by extraction
 with chloroform under both basic and acidic conditions.  Organic constituents
 were identified by gas chromatography/mass  spectrometry and quantified by gas-
 chromatographic techniques.  Inorganic constituents were determined by spark-
 source mass spectrometry, energy-dispersive x-ray fluorescence analysis,  and
 instrumental  neutron activation analysis.   For comparison with previous data from
 the  same sites, the samples were also analyzed for total chemical oxygen  demand,
 turbidity,  conductivity, pH, color, oxidation-reduction potential, suspended
 solids,  and volatile suspended solids.  Results of the inorganic analyses were
 presented in  previous quarterly progress  reports.   Final results of the organic
 analyses are  presented in this appendix to  the final  report.
17.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
 Water quality
 Water pollution
 Water analysis
 Water chemistry
 Surface waters
                                             b.IDENTIFIERS/OPEN ENDED TERMS
                Trace contaminants
                Organic compounds
                Volatile  organic
                    compounds
                Industrial  pollution
                Nationwide  survey
                                          c. COSATi l-'icld/Group
             8h
             7b,  7c,  7e
13. DISTRIBUTION1 STATEMENT
 Unrestricted
 Available  from National  Technical Infor-
 mation Service.  Springfield. VA  22151
               19. SECURITY CLASS (This Report)

                U nclassified	
               25. SECURITY CLASS (This page)

                Unclassified	
             21. NO. OF PAGES

               4	
             22. PRICE
EPA Form 2220-1 (9-73)

-------
EPA-560/7-77-001a
             MONITORING TO DETECT PREVIOUSLY  UNRECOGNIZED
                       POLLUTANTS  IN  SURFACE  WATERS

                    APPENDIX:  ORGANIC  ANALYSIS DATA
                     INSTITUTE FOR ENVIRONMENTAL STUDIES

                  University of Illinois at Urbana-Champaign
                       B. B. Ewing
                       E. S. K.  Chian
                  J. C. Cook
                  F. B. DeWalle
                  C. A. Evans
                  P. K. Hopke
                  J. H. Kim
Principal
Investigators


    J.  C. Means
       R. Mil berg
    E.  G. Perkins
    J.  D. Sherwood
    W.  H. Wadlin
                                Final Report
                           Contract  No. 68-01-3234
                                  July 1977
                     Project Officer—Vincent J. DeCarlo
                                Prepared for

                         Office of Toxic Substances
                     U.S. Environmental  Protection Agency
                           Washington, D.C.  20460
Document  is available to the public  through the National  Technical Information
                    Service, Springfield, Virginia  22151

-------
                                     NOTICE
     This report has been reviewed by the Office of Toxic Substances, EPA,
and approved for publication.  Approval  does not signify that the contents
necessarily reflect the views and policies of the Environmental  Protection
Agency,  nor  does mention  of trade names or commercial products constitute
endorsement or recommendation for use.

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                   1
               TABLE Bl
Organic Compounds Identified in Sample
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
Volatile Compounds
Dichloromethane
Acetone
Chloroform
Trichloro-trifluoroethane
Trichloroethylene
Benzene
Tetrachloroethyl ene
Toluene
Approximate
Level (PPB)
1
2
30
5
4
3
2
2

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               TABLE B2
Organic Compounds Identified in Sample # 1A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
Relative
Retention
Time
0.435
0.780
0.792
0.826
0.893
0.926
0.954
0.978
1.000
1.049
1.061
1.088
1.095
1.131
1.143
1.186
1.216
1.232
1.265
1.323
1.348
1.366
1.388
1.403
1.418
1.451
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C = 12
Methyl Trichlorophenyl Ether
Methyl Tetrachlorophenyl Ether
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Fatty Acid Methyl Ester C > 15
+ Methyl Pentachlorophenyl Ether
Fatty Acid Methyl Ester C >_ 15
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Dibutyl Phthalate
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 19
Fatty Acid Methyl Ester C >_ 20
?
Fatty Acid Methyl Ester C ^ 22
Fatty Acid Methyl Ester C >_ 22
Di ethyl Hexyl Phthalate
?
?
C,c - Terpineol
?
Fatty Acid Methyl Ester C > 26
?
Approximate
Level (PPB)
_ _ _
10
1
5
9
12
8 (mix)
2
45
4
4
14
43
4
4
11
35
6
15
14
14
7
6
7
2
4

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                TABLE B3
  Organic  Compounds  Identified  in  Sample  #1B
Relative
Retention
Peak # Time
1
2
3
4
5
6

Compounds in Base Extract
Xylene
Dibromo-chl oroethane
Camphor (IS)
Diisobutyl Phthalate
Dibutyl Phthalate
Terpineol

Approximate
Level (PPB)
19
14
—
1
1
1
               TABLE B4
Organic Compounds Identified in Sample # 2S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
Volatile Compounds
Acetone
Chloroform
Trichloro-trifluoroethane
Trichloroethane
Bromo-dichloromethane
Trichloroethylene
Benzene
Di bromo-chl oromethane
Tetrachloroethylene
Fluoro-dichloro-bromomethane
Toluene
Approximate
Level (PPB)
2
5
2
1
9
2
4
2
1
1
2

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                TABLE  B5
Organic Compounds Identified in Sample # 2A
Peak #
1
2
3
4
5
6
Relative
Retention
Time
0.467
0.899
1.000
1.105
1.319
1.386
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
—
2
4
2
1
1
               TABLE B6
  Organic Compounds  Identified in Sample #2B
Peak #
1
2
3
4
Relative
Retention
Time
—
—
—
—
Compounds in Base Extract
Tetrachloroethane
1 ,2-Diethoxyethane
Camphor (IS)
Terpineol
Approximate
Level (PPB)
2
2
—
2

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               TABLE  B7
Organic Compounds Identified in Sample #3S
Peak #
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time Volatile Compounds
— Dichloromethane
— Acetone
— Trichloro-fluoromethane
— Chloroform
— Trifluoro-trichloroethane
— Butane
— Trichloroethylene
— Benzene
— Tetrachloroethylene
— Toluene
— Chlorobenzene
Approximate
Level (PPB)
1
3
6
8
3
6
4
2
1
1
1

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                TABLE B8
Organic Compounds Identified in Sample # 3A

Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14



Peak i
1
2
3
4
5
Relative
Retention
Time
0.519
1.000
1.055
1.085
1.091
1.131
1.167
1.179
1.213
1.262
1.319
1.349
1.365
1.402

Organic
Relative
Retention
Time
—
—
—
—
—

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Dibutyl Phthalate
Methyl Stearate
?
?
Fatty Acid Methyl Ester C i 20
?
?
Diethyl Hexyl Phthalate
?
?
?
TABLE B9
Compounds Identified in Sample #3B

Compounds in Base Extract
Tetrachl oroethyl ene
Diethoxyethane
Dichlorobenzene
Camphor (IS)
?

Approximate
Level (PPB)
—
3
3
1
3
2
1
2
9
2
6
2
3
3



Approximate
Level (PPB)
2
3
4
	
1

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                                TABLE BIO

                Organic Compounds Identified in Sample # 4S
Peak 1
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time Volatile Compounds
— Dichloromethane
— Acetone
— Trichlorofluoromethane
— Chloroform
— Trichloro-trifluoroethane
— Pentane
— Trichloroethane
— Trichloroethylene
— Benzene
— Tetrachloroethylene
— Toluene
Approximate
Level (PPB)
2
3
6
9
3
2
1
2
1
1
1
                               TABLE Bll

               Organic Compounds Identified  in Sample # 4A
            Relative
           Retention                                          Approximate
Peak #       Time        Compounds in Acid Extract            Level (PPB)
            Sample 4A was destroyed and no quantitative data or
            chromatogram is available.

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                 8
              TABLE  B12
Organic Compounds Identified in Sample # 4B
Peak #
1
2
3
4
5


Peak #
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time Compounds in Base Extract
— Tetrachloroethylene
— Camphor (IS)
Naphthalene (IS)
Unidentified Phthalate
— Terpineol
TABLE B13
Organic Compounds Identified in Sample # 5S
Relative
Retention
Time Volatile Compounds
— Dichloromethane
— Acetone
— Tetrahydrofuran
— Chloroform
— Trifluoro-trichloroethane
— Trichloroethane
— Trichloroethylene
— Benzene
— Hexane
— Tetrachloroethylene
— Toluene
— Chlorobenzene
Approximate
Level (PPB)
11.3
—
—
3
1


Approximate
Level (PPB)
2
2
1
100
1
1
6
2
1
4
1
1

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                 TABLE B14
Organic Compounds Identified in Sample # 5A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Relative
Retention
Time
0.444
0.559
0.894
0.927
0.951
1.000
1.036
1.058
1.097
1.182
1.219
1.265
1.326
1.349
1.365
1.386
1.402
1.419
1.453
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Camphor
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
Hydrocarbon C ^ 18
?
Methyl Stearate
Fatty Acid Methyl Ester C ^ 20
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
?
?
?
?
?
7
Approximate
Level (PPB)
—
8
2
1
2
12
1
4
9
2
18
5
8
8
7
1
2
2
2

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                  10
               TABLE B15
 Organic Compounds Identified in Sample # 5B
Relative
Retention
Peak # Time
1
2
3
4
5
6
Compounds in Base Extract
Tetrachloroethylene
Diethoxyethane
Camphor (IS)
?
Diethyl-Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
2
4
—
1
1
1
               TABLE B16
Organic Compounds Identified in Sample # 6S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
n
12
13
14
Volatile Compounds
Dichloromethane
Acetone
Tetrahydrofuran
Chloroform
Dioxane
Pentane
Trichloroethylene
Benzene
Hexane
Diisopropyl Ether
Tetrachloroethylene
Toluene
Ethyl benzene
Dichlorobenzene
Approximate
Level (PPB)
2
4
1
1
1
1
6
2
1
1
4
2
1
1

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                  11
               TABLE  B17
Organic Compounds Identified in Sample # 6A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14


Peak #
1
2
3
4
5
6
Relative
Retention
Time
0.463
0.791
0.878
0.900
0.933
0.955
1.000
1.060
1.097
1.184
1.218
1.264
1.318
1.342

Organic
Relative
Retention
Time
—
—
—
—
—
—
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C = 12
Fatty Acid Methyl Ester C >_ 13
Fatty Acid Methyl Ester C = 14
Fatty Acid Methyl Ester C >_ 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 20
Fatty Acid Methyl Ester C >_ 21
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
TABLE B18
Compounds Identified in Sample #6B
Compounds in Base Extract
Tetrachl oroethyl ene
Diethoxyethane
Camphor (IS)
?
Diethyl Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
—
1
1
1
2
1
10
2
8
1
6
1
1
2


Approximate
Level (PPB)
3
5
—
1
1
4

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                   12
                TABLE B19
Organic Compounds Identified in Sample #7S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
Volatile Compounds
?
Dichloromethane
Acetone
Butene
Trichloro-trifluoroethane
Dichloroethylene
Cyclopentane
Tetrahydrofuran
Diethyl Ether
Chloroform
Pentane
Hexene
Trichloroethylene
Benzene
Hexane
Tetrachloroethylene
Toluene
Acetophenone
Chlorobenzene
Nonene
Ethyl benzene
Approximate
Level (PPB)
1
30
2
2
30
2
4
1
5
30
9
5
10
7
10
1
5
2
2
1
4

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                   13

                TABLE B20
Organic Compounds Identified in Sample # 7A

Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18



Peak #
Relative
Retention
Time
0.558
0.766
0.851
0.919
0.962
1.000
1.049
1.081
1.143
1.151
1.177
1.210
1.215
1.239
1.270
1.332
1.365
1.386

Organic
Relative
Retention
Time

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C,Q - Terpineol
Methyl -2(4-chlorophenoxy) Butanoate
Methyl Myri state
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 20
?
?
Fatty Acid Methyl Ester C >_ 22
Butyl benzyl Phthalate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
?
?
TABLE B21
Compounds Identified in Sample # 7B

Compounds in Base Extract

Approximate
Level (PPB)
— — —
1
1
1
3
5
5
11
1
1
11
2
2
2
2
1
1
1



Approximate
Level (PPB)
1          1.000
2          1.180
              Naphthalene (IS)

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                                   14
                                TABLE  B22

                Organic Compounds  Identified  in  Sample  #8S  (Field Stripped)
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8 -
9
10
11
Volatile Compounds
Dichloromethane
Acetone
Trichlorofluoromethane
Chloroform
Pentane
Bromo-dichloromethane
Trichloroethylene
Benzene
Hexane
Toluene
Chlorobenzene
Approximate
Level (PPB)
2
2
4
6
6
4
2
2
5
1
1
                               TABLE B23

               Organic Compounds Identified in Sample #8A  (Field  Extracted)
            Relative
           Retention                                          Approximate
Peak #       Time        Compounds in Acid Extract            Level (PPB)


   1        0.560        Methyl-2-ethyl Hexanoate (IS)

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                  15
              TABLE B24
Organic Compounds Identified in Sample #8B (Field Extracted)

Peak #
1



Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time Compounds in Base Extract
1.000 Naphthalene (IS)
TABLE B25
Organic Compounds Identified in Sample #8S
Relative
Retention
Time Volatile Compounds
— Dichloromethane
— Acetone
— Butene
— Trichloro-fluoromethane
— Chloroform
— Pentane
	 ?
	 ?
— Bromo-dichloromethane
— Hexane
— Benzene
— Dibromo-chloromethane
— Methyl Methacrylate
— Furfural
— Toluene
— Chlorobenzene

Approximate
Level (PPB)
—

(Lab Stripped)

Approximate
Level (PPB)
3
1
1
3
10
1
1
1
7
4
6
3
10
2
1
4

-------
                                  16
                              TABLE B26
               Organic Compounds Identified in Sample # 8A (Lab Extracted)
            Relative
           Retention                                          Approximate
Peak #       Time        Compounds in Acid Extract            Level (PPB)


   1        0.560        Methyl-2-ethyl  Hexanoate  (IS)
                              TABLE  B27
                Organic  Compounds  Identified  in  Sample  # 8B (Lab Extracted)
             Relative
            Retention                                        Approximate
 Peak #       Time          Compounds  in Base  Extract         Level  (PPB)

     1          1.000         Naphthalene (IS)

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                   17
                TABLE B28
Organic Compounds Identified in  Sample  #9S (Field Stripped)

Relative
Retention
Peak # Time

1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19

Volatile Compounds

Dichloromethane
Acetone
Butene
Tri chl oro-f 1 uoromethane
Dichloroethylene
Pentene Isomer
Tetrahydrofuran
Chloroform
Dichloroethane
Pentene Isomer
Trichloroethane
Pentane
Trichloroethylene
Benzene
Hexane
Methyl -isobutyl Ketone
Tetrachl oroethyl ene
Toluene
Ethyl benzene
Approximate
Level (PPB)
5
4
1
20
1
1
1
20
1
9
1
2
5
2
12
1
1
2
1

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                   18
                TABLE  B29
Organic Compounds Identified in Sample #9A (Field Extracted)

Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13



Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.556
0.854
0.911
1.000
1.048
1.081
1.104
1.149
1.176
1.208
1.258
1.277
1.312

Organic
Relative
Retention
Time
0.830
1.000
1.106
1.277
1.523
1.583
1.602
1.852
1.924

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl -2 (4-chlorophenoxy) Butanoate
Methyl Myri state
Methyl Palmitate
?
Methyl Stearate
Hydrocarbon C >_ 20
Hydrocarbon C > 22
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
C,r - Terpineol
TABLE B30
Compounds Identified in Sample #9B (

Compounds in Base Extract
Dichlorobenzene Isomer
Naphthalene (IS)
Alkyl Acid Ester (R + R1 > 8)
C,Q - Terpineol
?
Dibutyl Phthalate
Caffeine
Diethyl Hexyl Phthalate
C - Terpineol

Approximate
Level (PPB)
— _
1
2
6
2
10
1
1
11
2
3
6
8

Field Extracted)

Approximate
Level (PPB)
1
—
1
1
4
4
4
3
3
              15

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                   19
               TABLE B31
Organic Compounds Identified in Sample # 9S  (Lab  Stripped)
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Volatile Compounds
Dichloromethane
Acetone
Trichlorofluoromethane
Pentene
Tetrahydrofuran
Diethyl Ether
Chloroform
Pentane
Trichloroethane
Hexene
Trichloroethylene
Benzene
Hexane
Tetrachl oroethyl ene
Toluene
Ethyl Benzene
Approximate
Level (PPB)
8
4
20
1
1
3
20
10
1
2
4
1
10
1
2
2

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                   20
                TABLE  B32
Organic Compounds Identified in Sample # 9A  (Lab Extracted)

Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13


Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.558
0.850
0.911
1.000
1.035
1.081
1.149
1.176
1.208
1.240
1.250
1.277
1.312

Organic
Relative
Retention
Time
0.830
1.000
1.113
1.522
1.583
1.603
1.855
1.922

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl -2(4-chlorophenoxy) Butanoate
Methyl Myri state
Methyl Palmitate
?
Methyl Stearate
Hydrocarbon C >_ 22
?
Fatty Acid Methyl Ester C 1 22
Butyl benzyl Phthalate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C 1 24
C-c - Terpineol
TABLE B33
Compounds Identified in Sample # 9B
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
Alkyl Acid Ester (R + R1 >_8)
?
Dibutyl Phthalate
Caffeine
Diethyl Hexyl Phthalate
C1K - Terpineol

Approximate
Level (PPB)
— — _
1
2
13
2
19
1
11
2
4
18
6
9

(Lab Extracted)
Approximate
Level (PPB)
1
—
1
4
4
4
2
2

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                   21
                TABLE B34
Organic Compounds Identified in Sample #10S
Relative
Retention
Peak i Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
Volatile Compounds
Dichloromethane
Acetone
Butene
Trichloro-fl uoromethane
Dichloroethylene
Pentene
Tetrahydrofuran
Diethyl Ether
Chloroform
Trifluoro-trichloroethane
Dichloroethane
Pentane
Trichloroethane
Dioxane
Hexene
Dichloropropane
Trichloroethylene
Benzene
Dibromo-chloromethane
Hexane
Tetrachloroethylene
Toluene
Chlorobenzene
Ethyl benzene
Approximate
Level (PPB)
15
6
1
20
1
1
6
8
20
1
1
10
8
1
2
2
10
2
1
12
4
2
1
1

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                     22
                  TABLE  835
  Organic Compounds Identified  in  Sample  # 10A

Peak #
1
2
3
4
5
6
7
8
9
10
11



Peak #
Relative
Retention
Time
0.545
0.916
1.000
1.040
1.050
1.080
1.150
1.170
1.210
1.260
1.318

Organic
Relative
Retention
Time

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Fatty Acid Methyl Ester C ^16
?
Methyl Stearate
Fatty Acid Methyl Ester C ^18
?
Fatty Acid Methyl Ester C >_ 20
Diethyl Hexyl Phthalate
C,r - Terpineol
TABLE B36
Compounds Identified in Sample #10B

Compounds in Base Extract

Approximate
Level (PPB)
—
6
104
7
15
180
23
28
8
7
8



Approximate
Level (PPB)
1.000         Naphthalene  (IS)

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                   23
                TABLE  B37
Organic Compounds Identified in Sample
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
Volatile Compounds
Dichloromethane
Acetone
Tetrahydrofuran
Diethyl Ether
Chloroform
Dichloroethane
Trichloroethane
Bromo-dichloromethane
Dichloropropane
Trichloroethylene
Benzene
Tetrachl oroethyl ene
Approximate
Level (PPB)
8
1
1
1
5
1
4
1
1
5
1
4

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                   24
                TABLE  B38
Organic Compounds Identified in Sample #11A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18


Peak #
1
2
Relative
Retention
Time
0.590
0.833
0.840
0.850
0.919
0.960
1.000
1.030
1.045
1.077
1.113
1.146
1.170
1.208
1.253
1.274
1.289
1.307

Organic
Relative
Retention
Time
1.000
1.862
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C = 12
Methyl Trichlorophenyl Ether
Methyl -2-(4-chlorophenoxy) Butanoate
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
+ Methyl Pentachlorophenoxy Ether
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 18
Methyl Arachidate
?
Fatty Acid Methyl Ester C >_ 20
Diethyl Hexyl Phthalate
?
?
C-.C Terpineol
TABLE B39
Compounds Identified in Sample # 11B
Compounds in Base Extract
Naphthalene (IS)
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
—
22
14
11
24
24 (mix)
94
12
26
131
10
27
49
32
23
25
17
21


Approximate
Level (PPB)
— — _
1

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                    25
                TABLE B40
Organic Compounds Identified in Sample #12S (Nonchlorinated)
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Volatile Compounds
Dichloromethane
Acetone
Butene
Tri chl oro-f 1 uoromethane
Dichloroethylene
Tetrahydrofuran
Diethyl Ether
Chloroform
Pentane
Trichloroethane
Dioxane
Tetrahydropyran
Tri chl oroethy 1 ene
Benzene
CrHgO or C,H,,,0
Methyl -tetrahydropyran
Cu fi r\v* c u n
c 1 n c i o
Tetrachloroethylene
Toluene
Acetophenone
Approximate
Level (PPB)
3
1
3
5
1
3
10
20
6
4
1
9
4
1
10
2
4
5
1
1

-------
                   26
                TABLE B41
Organic Compounds Identified in Sample #12S (Chlorinated)
Relative
Retention
Peak i Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
Volatile Compounds
Dichloromethane
Acetone
Butene
Trichloro-fluoromethane
Dichloroethylene
Tetrahydrofuran
Di ethyl Ether
Chloroform
?
Pentane
Trichloroethane
Dioxane
Tetrahydropyran
Trichloroethylene
Benzene
Dimethyl formamide
CgHgO or CgH,20
Methyl -tetrahydropyran
C5H1Q0 or C6H]20
N ,N-Dimethyl acetamide
Tetrachloroethylene
Dichlorobenzene Isomer
Dichlorobenzene Isomer
Approximate
Level (PPB)
3
2
5
4
1
4
10
14
1
2
6
2
9
4
2
2
14
4
6
2
4
2
2

-------
                   27
                TABLE  B42
Organic Compounds Identified in Sample # 12A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
Relative
Retention
Time
0.572
0.670
0.717
0.753
0.768
0.830
0.854
0.917
0.943
0.964
1.000
1.040
1.047
1.077
1.112
1.137
1.148
1.175
1.208
1.261
i:277
1.294
1.312
1.324
1.335
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
Methyl Dichlorophenyl Ether
?
Methyl Trichlorophenyl Ether
C,n - Terpineol
Fatty Acid Methyl Ester C = 12
Methyl -2- (4-chlorophenoxy) Butanoate
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Methyl Stearate
?
?
Methyl Arachidate
?
Fatty Acid Methyl Ester C >_ 22
+ Methyl Dehydroabietate
Diethyl Hexyl Phthalate
7
7
7
7
7

5
8
10
15
4
4
18
31
26
117
19
27
173
24
23
25
60
90 (mix)
137
50
68
50
52
68

-------
                     28
                 TABLE 843
   Organic  Compounds  Identified  in  Sample  #  12B
Peak if
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.810
1.000
1.103
1.620
1.699
1.754
1.830
1.873
1.952
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
Alkyl Acid Ester (R + R1 >_ 8)
Caffeine
?
?
?
Diethyl Hexyl Phthalate
C,5 - Terpineol
Approximate
Level (PPB)
16
—
2
1
9
4
2
1
1
                TABLE B44
Organic Compounds Identified in Sample # 13S
Peak #
1
2
3
4
5
Relative
Retention
Time

—
—
—
— _
Volatile Compounds
Chloroform
Bromo-dichloromethane
Trichloroethylene
Benzene
Chi oro benzene
Approximate
Level (PPB)
8
4
2
3
1

-------
                               29
                            TABLE B45
             Organic Compounds Identified in Sample #13A
Peak #
1
2
3
4
Relative
Retention
Time
0.545
1.000
1.263
1.320
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
Diethyl Hexyl Phthalate
C,j. - Terpineol
Approximate
Level (PPB)
_ _ _
1
1
1
                            TABLE B46
              Organic Compounds Identified in Sample #13B
           Relative
           Retention                                        Approximate
Peak #       Time         Compounds in Base Extract         Level  (PPB)

   1        1.000         Naphthalene (IS)

-------
                   30
                TABLE B47
Organic Compounds Identified in Sample # 14S

Peak #
1
2
3
4
5
6
7
8
9
10
11



Peak #
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time
— _
—
—
—
—
—
—
—
—
—
—

Organic
Relative
Retention
Time
0.557
0.853
0.902
0.919
0.940
1.000
1.078
1.138
1.260
1.293
1.423
1.447

Volatile Compounds
Trichloro-fluoromethane
Neopentane
Chloroform
Trichloroethane
Hexene Isomer
Hexene Isomer
1-Bromo-l-chloroethane
Benzene
Dibromoethane
Methyl -isobutyl Ketone
Heptene
TABLE B48
Compounds Identified in Sample # 14A

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Hydrocarbon C > 16
Hydrocarbon C > 18
Fatty Acid Methyl Ester C ^ 14
Hydrocarbon C > 18
Methyl Palmitate
Methyl Stearate
ci6Hio (pyrene?)
Diethyl Hexyl Phthalate
(C,gH12) Benzanthrene
?
?

Approximate
Level (PPB)
1
2
1
2
1
1
1
1
10
2
1



Approximate
Level (PPB)
—
2
2
2
1
2
5
1
1
1
8
8

-------
                  31
               TABLE B49
Organic Compounds Identified  in  Sample  #148
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.474
1.000
1.235
1.270
1.346
1.625
1.657
1.708
1.741
1.856
1.887
1.944
1.968
Compounds in Base Extract
Dibromoethane
Naphthalene (IS)
Hydrocarbon C >_ 16
Hydrocarbon C >_ 16
Hydrocarbon C ^ 18
Caffeine
Hydrocarbon C >_ 22
Hydrocarbon C >_ 22
ci6Hio (pyrene)
Benzylbutyl Phthalate
Di ethyl Hexyl Phthalate
Hydrocarbon C >_ 28
Terpineol
Approximate
Level (PPB)
6
—
1
1
1
2
1
1
1
1
4
1
4

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                    32
                TABLE B50
Organic Compounds Identified in Sample # IBS

Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13



Peak #
1
2
3
4
5
Relative
Retention
Time
—
—
—
—
—
—
—
—
—
—
—
—
—

Organic
Relative
Retention
Time
0.575
1.000
1.060
1.250
1.300

Volatile Compounds
Dichloromethane
Acetone
Trichloro-fl uoromethane
Dichloroethylene
Chloroform
Pentane
Dichloroethane
Trichloroethane
Hexene
Trichloroethylene
Benzene
Tetrachloroethylene
• Chlorobenzene
TABLE B51
Compounds Identified in Sample # ISA

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Pa Imitate
Methyl Stearate
Diethyl Hexyl Phthalate
C,r - Terpineol

Approximate
Level (PPB)
1
1
1
2
1
1
6
1
4
6
2
3
1



Approximate
Level (PPB)
—
1
1
5
4

-------
                                33
                            TABLE B52

              Organic Compounds Identified in Sample # 15B
           Relative
           Retention                                        Approximate
Peak #       Time         Compounds in Base Extract         Level  (PPB)


   1        1.000         Naphthalene (IS)
                            TABLE B53

            Organic Compounds Identified in Sample #16S
Relative
Retention
Peak # Time
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Volatile Compounds
Dichloromethane
Acetone
Butene
Trichloro-fluoromethane
Dichloroethylene
Diethyl Ether
Chloroform
Pentane
Tetrahydropyran
Trichloroethylene
Benzene
Hexane
Tetrachl oroethyl ene
Toluene
Chlorobenzene
Approximate
Level (PPB)
2
1
1
12
2
5
20
8
3
5
4
10
4
2
1

-------
                    34
                TABLE B54
Organic Compounds Identified in Sample # 16A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.579
0.770
0.850
0.900
0.920
0.960
1.000
1.040
1.044
1.070
1.140
1.170
1.210
1.250
1.257
1.270
1.280
1.300
1.320
1.330
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
C,n - Terpineol
Hydrocarbon C > 18
+ Methyl -2(4-chlorophenoxy) Butanoate
Fatty Acid Methyl Ester C >. 14
Fatty Acid Methyl Ester C >_ 14
Fatty Acid Methyl Ester C > 14
+ Methyl Pentachlorophenyl Ether
Methyl Palmitate
Fatty Acid Methyl Ester C i 16
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 18
?
Fatty Acid Methyl Ester C >_ 20
Di ethyl Hexyl Phthalate
?
?
?
?
?
?
—
10
10 (mix)
21
20
25 (mix)
70
9
29
79
34
85
33
50
25
35
25
30
43
41

-------
                    35
                TABLE B55
  Organic Compounds  Identified  in Sample #  16B
Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.811
1.000
1.102
1.429
1.594
1.618
1.873
1.952
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
C,0 - Terpineol
Dimethyl Biphenyl
Di butyl Phthalate
Caffeine
Di ethyl Hexyl Phthalate
C - Terpineol
15
Approximate
Level (PPB)
18
—
1
1
1
1
1
1
              TABLE B56
Organic Compounds Identified in Sample ti 17S

Peak #
1
2
Relative
Retention
Time
0.548
1.000

Volatile Compounds
Dichloromethane
Chloroform

Approximate
Level (PPB)
1
2

-------
                  36
               TABLE 857
Organic Compounds Identified  in Sample  #17A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time
0.563
0.739
0.763
0.846
0.913
1.959
1.000
1.062
1.075
1.113
1.175
1.207
1.213
1.261
1.277
1.312
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Trichlorophenyl Ether
C,Q - Terpineol
Methyl -2 (4-chlorophenoxy) Butanoate
Fatty Acid Methyl Ester C = 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
?
Methyl Dehydroabietate
Butyl phthalyl butyl Glycolate
Di ethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
C,r - Terpineol
Approximate
Level (PPB)
—
12
10
10
7
43
81
10
45
55
45
37
48
85
52
104

-------
                    37
                TABLE B58
  Organic Compounds Identified in Sample # 17B
Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.812
1.000
1.112
1.463
1.623
1.843
1.887
1.963
Compounds in Base Extract
Dichlorobenzene
Naphthalene (IS)
C.Q - Terpineol
?
Caffeine
?
Di ethyl Hexyl Phthalate
Terpineol
Approximate
Level (PPB)
4
—
1
1
2
1
1
1
                 TABLE B59
Organic Compounds Identified in Sample # 18S
Peak 1
1
2
3
4
Relative
Retention
Time
1.000
1.307
1.569
2.126
Volatile Compounds
Chloroform
Bromo-dichloromethane
Dibromo-chloromethane
Toluene
Approximate
Level (PPB)
13
2
4
1

-------
                    38
                TABLE B60
Organic Compounds Identified  in Sample #  ISA
Peak #
1
. 2
3
4
Relative
Retention
Time
0.453
0.828
1.000
1.098
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C,n - Terpineol
Methyl Palmitate
Methyl Stearate
Approximate
Level (PPB)
—
1
1
1
                TABLE B61
Organic Compounds Identified in Sample # 18B
Peak #
1
2
3
4
Relative
Retention
Time
1.000
1.492
1.968
2.385
Compounds in Base Extract
Camphor (IS)
C-.Q - Terpineol
Dibutyl Phthalate
Diethyl Phthalate
Approximate
Level (PPB)
—
3
1
4

-------
                                  39


                              TABLE B62

              Organic Compounds Identified in Sample #  19S
            Relative                                         ....
           Retention                                        Approximate
Peak #       Time         Volatile Compounds                Level (PPB)
              Sample #19 was not assayed for volatiles.

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                  40
               TABLE B63
Organic Compounds Identified in Sample #19A
Peak §
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Relative
Retention
Time
0.550
0.817
0.890
0.948
1.000
1.024
1.064
1.106
1.131
1.143
1.188
1.213
1.234
1.277
1.286
1.316
1.347
1.372
1.396
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C10 - Terpineol
Methyl Myri state
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
?
Methyl Stearate
?
Hydrocarbon C >_ 22
Hydrocarbon C > 24
?
?
Methyl Dehydroabietate
Fatty Acid Methyl Ester C >_ 22
Hydrocarbon C > 26
Di ethyl Hexyl Phthalate
?
Hydrocarbon C > 30
Approximate
Level (PPB)
— — •
7
5
10
61
8
5
56
17
18
20
19
52
15
35
22
38
27
20

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                   41
                TABLE B64
 Organic Compounds Identified in Sample #19B
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.511
2.011
2.175
2.258
2.351
2.461
Compounds in Base Extract
Camphor (IS)
C,Q - Terpineol
Dibutyl Phthalate
Hydrocarbon C > 22
Hydrocarbon C > 24
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
—
2
4
1
1
3
1
                TABLE  B65
Organic Compounds Identified in Sample # 20S
Peak #
1
2
3
Relative
Retention
Time
1.000
1.533
2.221
Volatile Compounds
Chloroform
Benzene
Chlorobenzene
Approximate
Level (PPB)
12
2
1

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                                 42
                              TABLE B66
               Organic  Compounds  Identified  in  Sample  #  20A
Peak #
1
2
3
Relative
Retention
Time
0.455
1.100
1.093
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level (PPB)
—
1
1
                             TABLE  B67
              Organic Compounds Identified in Sample #20B
Peak #
Relative
Retention
  Time
Compounds in Base Extract
                                                            Approximate
                                                            Level  (PPB)
            1.000
               Camphor (IS)

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                   43
                TABLE B68
Organic Compounds Identified in Sample # 21S
Peak i
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.862
1.000
1.085
1.195
1.303
1.515
1.543
1.978
2.036
2.127
Volatile Compounds
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Tetrahydropyran
Trichloroethylene
Benzene
Dichlorobenzene
Tetrachloroethylene
Toluene
Approximate
Level (PPB)
1
16
1
3
2
1
1
1
2
1

-------
                 44
              TABLE B69
Organic Compounds Identified in Sample # 21A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
Relative
Retention
Time
0.499
0.666
0.899
1.000
1.048
1.058
1.091
1.131
1.170
1.179
1.200
1.215
1.254
1.261
1.315
1.346
1.361
1.379
1.400
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Hydrocarbon C >_ 14
Methyl Myri state
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
?
Methyl Stearate
?
C16H10 lsomer
Fatty Acid Methyl Ester C >_ 20
C,nH,n Isomer
? •
Methyl Dehydroabietate
Fatty Acid Methyl Ester
Diethyl Hexyl Phthalate
?
?
?
?
Approximate
Level (PPB)
—
1
2
22
3
3
33
2
1
10
1
12
4
5
20
8
6
5
2

-------
                   45
                TABLE B70
Organic Compounds Identified in Sample #21B
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.405
2.384
2.455
2.701
2.739
2.799
Compounds in Base Extract
Camphor (IS)
Hydrocarbon C > 16
Di ethyl Hexyl Phthalate
C18H12
?
?
?
Approximate
Level (PPB)
- _ _
1
7
1
1
8
6
                TABLE  B71
Organic Compounds Identified in  Sample  #22S
Peak #
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.485
0.867
1.000
1.072
1.172
1.393
1.481
1.985
Volatile Compounds
Acetone
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
1 ,2-Dichloropropane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level (PPB)
2
1
22
1
1
2
7
1

-------
                    46
                TABLE B72
Organic Compounds Identified in Sample #  22A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.438
0.787
0.797
0.815
0.827
0.897
0.951
1.000
1.018
1.057
1.097
1.185
1.218
1.263
1.318
1.324
1.339
1.364
1.385
1.400
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
Fatty Acid Methyl Ester C >_ 12
Methyl Trichlorophenyl Ether
Methyl -2(4-chlorophenoxy) Butanoate
Methyl Tetrachlorophenyl Ether
Methyl Myri state
Methyl Pentachlorophenyl Ether
Methyl Palmitate
Alkyl Benzene
?
Methyl Stearate
Fatty Acid Methyl Ester C ^ 20
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
7
?
?
C,5 ~ Terpineol
?
—
1
1
1
2
1
1
2
1
2
3
1
8
4
2
2
2
1
1
1

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                  47
               TABLE B73
Organic Compounds Identified in Sample # 22B

Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13



Peak i
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.313
1.526
1.609
1.755
1.800
1.889
2.007
2.097
2.147
2.208
2.302
2.432

Organic
Relative
Retention
Time
0.427
0.861
0.959
1.000
1.087
1.197
1.434
1.527
2.054

Compounds in Base Extract
Camphor (IS)
Hydrocarbon
?
?
Diphenyl Ethane
Alkyl Phenyl Ether
?
Dibutyl Phthalate
?
C16H10
C16H10
?
Diethyl Hexyl Phthalate
TABLE B74
Compounds Identified in Sample ft 23S

Volatile Compounds
Dichloromethane
Tetrahydrofuran
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
1 ,2-Dichloropropane
Trichloroethylene
Tetrachloroethylene

Approximate
Level (PPB)
—
1
3
3
3
4
2
1
1
1
3
2
5



Approximate
Level (PPB)
1
2
1
27
2
1
1
5
1

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                   48
               TABLE B75
 Organic Compounds  Identified  in Sample #23A
Peak #
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time
0.446
0.814
0.897
0.951
0.969
1.000
1.057
1.097
1.215
1.264
1.326
1.347
Approximate
Compounds in Acid Extract Level (PPB)
Methyl -2-ethyl Hexanoate (IS)
Methyl -2(4-chlorophenoxy) Butanoate
Fatty Acid Methyl Ester C = 14
Fatty Acid Methyl Ester C >_ 14
Alkyl Benzene
Methyl Palmitate
?
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 22
Di ethyl Hexyl Phthalate
?
	
2
2
2
3
2
2
3
6
3
1
2
               TABLE  B76
Organic Compounds Identified in Sample #23B
Peak #
1
2
3
4
Relative
Retention
Time
1.000
1.963
2.275
2.374
Compounds in Base Extract
Camphor (IS)
Di butyl Phthalate
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
_ _ _
2
6
2

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                  49
               TABLE B77
Organic Compounds Identified in Sample # 24S


Peak #
1
2
3
4
5
6



Peak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Relative
Retention
Time
0.954
1.000
1.075
1.184
1.512
2.036

Organic
Relative
Retention
Time
0.436
0.812
0.933
0.952
1.000
1.057
1.094
1.215
1.254
1.269
1.318
1.342
1.363
1.384
1.403
1.436
1.463


Volatile Compounds
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
Tetrachloroethylene
TABLE B78
Compounds Identified in Sample # 24A

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl -2(4-chlorophenoxy) Butanoate
Hydrocarbon C >_ 16
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
?
?
Di ethyl Hexyl Phthalate
?
Hydrocarbon C >_ 28
C,,- - Terpineol
1 D
Hydrocarbon C ^ 30
Hydrocarbon C >_ 30
Hydrocarbon C >_ 30

Approximate
Level (PPB)
1
17
1
1
2
2


Approximate
Level (PPB)
—
2
1
1
2
2
3
9
3
1
1
3
1
1
1
1
1

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                     50
                  TABLE B79
   Organic Compounds Identified in Sample # 24B
Peak #
1
2
3
4
5
Relative
Retention
Time
1.000
1.991
2.356
2.411
2.522
Compounds in Base Extract
Camphor (IS)
Dibutyl Phthalate
Butyl benzyl Phthalate
Diethyl Hexyl Phthalate
C,r - Terpineol
Approximate
Level (PPB)
—
2
1
1
1
                  TABLE B80
Organic Compounds Indentified  in  Sample # 25S
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
0.864
0.954
1.000
1.079
1.187
1.493
1.998.
Volatile Compounds
Tetrahydrofuran
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level (PPB)
2
1
26
1
1
1
1

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                   51
                TABLE B81
Organic Compounds Identified in Sample # 25A
Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.448
1.000
1.058
1.094
1.206
1.254
1.321
1.346
1.385
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
?
Diethyl Hexyl Phthalate
?
C,r - Terpineol
Approximate
Level (PPB)
—
2
2
3
6
2
1
2
2
               TABLE B82
 Organic Compounds Identified in Sample #25B

Peak #
1
2
3
Relative
Retention
Time
1.000
2.013
2.441

Compounds in Base Extract
Camphor (IS)
Dibutyl Phthalate
Diethyl hexyl Phthalate

Approximate
Level (PPB)
— _ _
1
1

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                   52
               TABLE B83
Organic Compounds Identified in Sample # 26S

Peak #
1
2
3
4
5
6
7



Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.396
0.957
1.000
1.141
1.483
1.509
1.983

Organic
Relative
Retention
Time
0.468
0.951
1.000
1.057
1.094
1.215
1.322
1.347
1.386

Volatile Compounds
Dichloromethane
Dichloroethylene
Chloroform
1 ,1 ,1-Trichloroethane
Trichloroethylene
Benzene
Tetrachl oroethyl ene
TABLE B84
Compounds Identified in Sample # 26A

Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Pentachlorophenyl Ether
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
?
C,c - Terpineol

Approximate
Level (PPB)
1
1
20
1
1
1
1



Approximate
Level (PPB)
	 	
1
2
1
3
4
2
2
2

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                                53
                             TABLE  B85
              Organic Compounds Identified in Sample #26B
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.985
2.413
2.441
2.530
2.647
2.780
Compounds in Base Extract
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
?
C,r - Terpineol
?
?
Approximate
Level (PPB)
— — —
1
2
1
4
2
2
                                TABLE B86
              Organic Compounds Identified in Sample # 27S
           Relative
           Retention                                         Approximate
Peak i       Time         Volatile Compounds                Level  (PPB)

   1         1.000        Chloroform                             14

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                   54
                TABLE B87
Organic Compounds  Identified  in Sample #27A
Peak #
1
2
3
4
5
6
Relative
Retention
Time
0.468
0.960
1.000
1.097
1.222
1.319
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
C Cl F n * 4
n x z -
Methyl Palmitate
Methyl Stearate + C Cl F , n % 4
II n £
C Cl F n ^ 4
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
—
2
1
4 (mix)
2
1
               TABLE  B88
Organic Compounds Identified in Sample # 27B
Peak #
1
2
3
4
Relative
Retention
Time
1.000
1.977
2.397
2.513
Compounds in Base Extract
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C1(; - Terpineol
Approximate
Level (PPB)
—
2
1
1

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                  55
               TABLE B89
Organic Compounds Identified in Sample # 28S
Peak #
1
2
3
4
5
6


Peak #
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
1.000
1.189
• 1.516
1.544
2.031
2.123

Organic
Relative
Retention
Time
0.464
0.907
0.945
1 . 000
1:058
1.095
1.221
1.329
1.357
1.375
1.397
Volatile Compounds
Chloroform
1 ,1 ,1-Trichloroethane
Trichloroethylene
Benzene
Tetrachloroethylene
Toluene
TABLE B90
Compounds Identified in Sample # 28A
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
7
Methyl Pentachlorophenyl Ether
Methyl Palmitate
7
Methyl Stearate
7
Diethyl Hexyl Phthalate
7
7
C1C - Terpineol
Approximate
Level (PPB)
18
1
1
1
1
1


Approximate
Level (PPB)
— — —
2
1
2
2
3
4
2
2
1
1

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                                 56
                              TABLE  B91

               Organic Compounds Identified in Sample #28B
Peak #
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.499
1.991
2.326
2.432
2.466
Compounds in Base Extract
Camphor (IS)
CIQ - Terpineol
Dibutyl Phthalate
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
?
Approximate
Level (PPB)
...
1
1
2
3
3
                             TABLE B92
              Organic Compounds Identified  in Sample # 29S
            Relative
           Retention                                        Approximate
Peak #       Time         Volatile Compounds                Level (PPB)


   1        1.000         Chloroform                             14
   2        1.504         Trichloroethylene                       1
   3        1.532         Benzene                                 1

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                   57
               TABLE B93
Organic Compounds Identified in Sample # 29A
Peak #
1
2
3
4
5
6
7



Peak #
1
2
3
4
5
Relative
Retention
Time
0.451
1.000
1.056
1.096
1.223
1.325
1.394

Organic
Relative
Retention
Time
1.000
1.962
2.386
2.413
2.502
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
C,r - Terpineol
TABLE B94
Compounds Identified in Sample #29B

Compounds in Base Extract
Camphor (IS)
Di butyl Phthalate
Diethyl Hexyl Phthalate
?
Terpineol
Approximate
Level (PPB)
—
2
1
2
3
1
1



Approximate
Level (PPB)
...
1
1
1
2

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                   58
                TABLE B95
Organic Compounds Identified in Sample #30S

Peak #
1
2
3
4
5
Relative
Retention
Time
1.000
1.262
1.507
1.535
2.230

Volatile Compounds
Chloroform
?
Trichloroethylene
Benzene
Acetophenone

Approximate
Level (PPB)
120
10
1
1
1
               TABLE B96
Organic Compounds Identified in Sample #30A
Peak #
1
2
3
4
5
6
7
Relative
Retention
Time
0.442
1.000
1.058
1.094
1.215
1.321 .
1.385
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
C c - Terpineol
Approximate
Level (PPB)
—
1 ,
1
2
3
1
1

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                                 59
                             TABLE B97
              Organic Compounds  Identified  in Sample #30B
            Relative
           Retention                                        Approximate
Peak #       Time         Compounds in Base Extract         Level (PPB)

    1         1.000         Camphor  (IS)
    2         1.995         Dibutyl  Phthalate                       1
    3         2.422         Diethyl  hexyl Phthalate                 1
    4         2.457         ?                                       1
                             TABLE B98
              Organic Compounds Identified in Sample #31S
            Relative
           Retention                                        Approximate
Peak #       Time         Volatile Compounds                Level  (PPB)

   1        1.000         Chloroform                            14
   2        1.535         Trichloroethylene                      1
   3        1.564         Benzene                                1
   4        1.995         Tetrachloroethylene                    1

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                   60
               TABLE B99
Organic Compounds Identified in Sample i 31A
Peak #
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.442
0.551
0.567
0.607
1.000
1.092
1.215
1.261
1.316
Compounds in Acid Extract
Methyl -2-ethyl Hexanoate (IS)
?
?
?
Methyl Palmitate
Methyl Stearate
?
Butyl phthalyl butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level (PPB)
—
1
1
1
3
3
2
4
1
               TABLE B100
Organic Compounds  Identified in Sample # 31B
Peak #
1
2
3
Relative
Retention
Time
1.000
2.409
2.527
Compounds in Base Extract
Camphor (IS)
Diethyl Hexyl Phthalate
C,r - Terpineol
Approximate
Level (PPB)
___
1
2

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                            61
                        TABLE B101
   Volatile Organic Compounds Identified in Sample No.  32S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.729
1.000
1.006
1.583
2.295
Compound
Dimethoxymethane
Chloroform
1 ,2-Dichloroethane
Benzene
Chlorobenzene
Approximate
Level
(ppb)
2
2
2
1
1
                        TABLE B102
Organic Compounds Identified in Acid Extract of Sample No. 32A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.464
1.000
1.094
1.265
1.322
1.386
1.450
1.526
Compound
Methyl -2-ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C-, 5 Terpineol
?
?
Approximate
Level
(ppb)
...
3
3
2
2
1
1
1

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                          62
                       TABLE B103
Organic Compounds Identified in Base Extract  of Sample  No.32B
Peak
No.
1
2
3
4
5
6
7
8
9


Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.107
1.207
1.237
1.521
2.043
2.398
2.511
2.648

Volatile
Relative
Retention
Time
0.735
0.868
1.000
1.081
1.524
2.047
Compound
Camphor (IS)
?
Nitrotoluene
Chloro-Nitrobenzene
C,Q - Terpineol
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C,5 - Terpineol
TABLE B104
Organic Compounds Identified in Sample No.
Compound
Dimethoxymethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
___
4
4
17
1
1
1
49
1

33S
Approximate
Level
(ppb)
1
1
2
1
1
1

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                           63
                       TABLE B105
Organic Compounds Identified in  Acid  Extract  of  Sample No.33A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.483
0.502
0.955
1.000
1.020
1.103
1.350
1.372
1.420
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
?
Methyl Palmitate
?
Methyl Stearate
Di ethyl Hexyl Phthalate
Fatty Acid Methyl Ester C > 22
C,r - Terpineol
Approximate
Level
(ppb)
_ _ _
1
25
4
1
3
1
1
2

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                          64
                       TABLE  B106
Organic Compounds Identified  in Base Extract of Sample  No.  33B
Peak
No.
1
2
3
4
5
6
7


Peak
No.
1
2
3
4
5
6

Relative
Retention
Time
0.827
1.000
1.101
1.208
1.244
1.657
2.514

Volatile
Relative
Retention
Time
0.719
0.862
1.000
1.086
1.532
2.053

Compound
Dichlorobenzene
Camphor (IS)
?
Nitrotoluene
Chloronitrobenzene
Dinitrotoluene
Diethyl Hexyl Phthalate
TABLE B107
Organic Compounds Identified in Sample No.
Compound
Dimethoxymethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
TABLE BIOS
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
Relative
Retention
Time
0.500
1.000
1.084
1.289
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
3
—
1
1
2
1
1

34S
Approximate
Level
(ppb)
3
1
2
12
2
3

N0.34A
Approximate
Level
(ppb)
—
2
2
1

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                               65
                            TABLE  B109
     Organic Compounds  Identified  in  Base  Extract of Sample No.  34B
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
2.037
2.499
2.630
Compound
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
C,c Terpineol
Approximate
Level
(ppb)
-. _ _
1
2
3
                            TABLE B110
       Volatile Organic Compounds Identified in Sample No. 35S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       0.749      Dimethoxymethane                             3
  2       1.000      Chloroform                                   2
  3       1.082      1,2-Dichloroethane                          15
  4       1.507      Trichloroethylene                            1
  5       2.004      Tetrachloroethylene                          3

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                               66
                           TABLE Bill

    Organic Compounds Identified in Acid Extract of Sample No.35A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.490
1.000
1.102
1.349
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— — _
2
2
1
                           TABLE B112
    Organic Compounds Identified in Base Extract of Sample No. 35B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


                   No peaks over 1 PPB.
                           TABLE B113
       Volatile Organic Compounds  Identified  in  Sample  No.  36S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.710
1.000
1.069
1.535
2.063
Compound
Dimethoxymethane
Chloroform
1,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
3
7
9
1
2

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                               67
                           TABLE B114
    Organic Compounds Identified in Acid Extract of Sample  No.  36A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0/450
0.958
1.000
1.099
1.336
1.401
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C-.C - Terpineol
Approximate
Level
(ppb)
— - —
19
6
11
1
1
                           TABLE B115
    Organic Compounds  Identified in Base Extract of Sample No. 36B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.380      Diethyl Hexyl Phthalate                      1

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                               68
                           TABLE  B116
       Volatile Organic Compounds Identified in Sample No. 37S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.730
1.000
1.079
1.461
1.917
Compound
Dimethoxymethane
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
4
2
15
1
2
                            TABLE B117
    Organic Compounds Identified  in Acid Extract of Sample No. 37A

       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)

  1       0.453     Methyl-2-Ethyl Hexanoate  (IS)
  2       1.000     Methyl  Palmitate                             2
  3       1.098     Methyl  Stearate                              5

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                               69
                           TABLE B118
     Organic  Compounds  Identified in Base Extract of Sample No. 37B

Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.897
2.431


Compound
Camphor (IS)
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
2
1
                            TABLE B119
       Volatile Organic Compounds Identified in Sample No. 38S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       0.414      Dichloromethane                              2
  2       0.489      Acetone                                      2
  3       0.722      Dimethoxymethane                             2
  4       1.000      Chloroform                                   2
  5       1.087      1,2-Dichlorqethane                          11
  6       1.447      1,2-Dichloropropane                          1
  7       1.537      Trichloroethylene                            1
  8       1.568      Benzene                                      1
  9       2.050      Tetrachloroethylene                          1

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                               70
                           TABLE B120

    Organic Compounds Identified in Acid Extract  of Sample  No.  38A

Peak
No.
1
2
3
Relative
Retention
Time
0.450
1.000
1.096


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
— _
3
3
                           TABLE B121

    Organic Compounds Identified in Base Extract of Sample No.38B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


 1      1.000      Camphor (IS)

 2      1.627      ?                                            2

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                          71
                       TABLE B122
   Volatile  Organic Compounds  Identified in Sample No. 39S
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.491
0.759
1.000
1.077
1.175
1.394
1.509
1.973
2.061
Compound
Dichloromethane
Methyl al
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
1 ,2-Dichloropropane
Trichloroethylene
Tetrachl oroethyl ene
Toluene
Approximate
Level
(Ppb)
8
12
12
90
1
2
24
4
1
                       TABLE B123
Organic Compounds Identified in Acid Extract  of Sample  No.  39A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.452
1.000
1.095
1.327
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
6
8
1

-------
                               72
                           TABLE B124

     Organic  Compounds  Identified in Base Extract of Sample No.39B
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.572
1.627
1.991
2.249
2.431
2.508
2.684
2.833
Compound
Camphor (IS)
?
?
Dibutyl Phthalate
?
Diethyl Hexyl Phthalate
Unidentified Phthalate
?
?
Approximate
Level
(ppb)
— — _
1
3
1
1
1
1
1
1
                            TABLE B125

       Volatile Organic Compounds Identified in Sample No. 40S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   4

  2       1.524      Trichloroethylene                            2

  3       2.036      Tetrachloroethylene                          1

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                              73
                           TABLE B126
    Organic  Compounds  Identified  in  Acid  Extract  of Sample No. 40A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.467
1.000
1.099
1.329


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
2
3
1
                           TABLE B127
    Organic Compounds  Identified in Base Extract of Sample No. 40B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       1.612      ?                                            2
  3       2.416      Diethyl Hexyl Phthalate                      2
  4       2.662      ?                                            4
  5       2.790      ?                                            2

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                               74
                            TABLE B128
       Volatile Organic Compounds  Identified in Sample No. 41S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   6
  2       1.500      Trichloroethylene                            1
  3       2.054      Tetrachloroethylene                          1
                            TABLE B129
    Organic Compounds  Identified  in Acid Extract of Sample No. 41A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.472
1.000
1.093
1.326
1.458
1.517
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
?
?
Approximate
Level
(ppb)
—
6
6
2
4
3

-------
                               75
                            TABLE  B130
     Organic Compounds Identified  in Base  Extract  of  Sample  No.  41B

       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                  (ppb)

  1       1.000      Camphor (IS)
  2       1.612      ?                                            1
  3       2.420      Diethyl  Hexyl  Phthalate                       1
  4       2.662      ?                                            2
                            TABLE  B131
       Volatile Organic Compounds Identified in Sample No. 42S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1       1.000      Chloroform                                  13
 2       1.086      1,2-Dichloroethane                           8
 3       1.507      Trichloroethylene                            4
 4       2.053      Tetrachloroethylene                          5

-------
                               76
                           TABLE B132
    Organic Compounds  Identified  in  Acid  Extract  of  Sample  No.  42A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.450
1.000
1.096
1.331
1.397
1.466
1.546
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C,5 - Terpineol
?
?
Approximate
Level
(PPb)
___
5
6
1
1
2
2
                           TABLE B133
    Organic Compounds  Identified in Base Extract of Sample No. 42B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

 1      0.850      Dichlorobenzene                              3
 2      1.000      Camphor (IS)
 3      1.102      Nitrotoluene                                 7
 4      1.236      Chloronitrobenzene                          13
 5      2.381      Diethyl Hexyl Phthalate                      1
 6      2.622      ?                                            3
 7      2.772      ?                                            3

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                           77
                       TABLE B134
   Volatile Organic Compounds Identified in Sample No.  43S
Peak
No.
1
2
3
Relative
Retention
Time
0.535
1.000
1.505
Compound
Acetone
Chloroform
Trichloroethylene
Approximate
Level
(ppb)
1
2
2
                       TABLE B135
Organic Compounds Identified in Acid Extract of Sample No.  43A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.450
1.000
1.097
1.200
1.240
1.333
1.352
1.379
1.400
1.467
1.549
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
?
Dioctyl Adipate
Di ethyl Hexyl Phthalate
Diethyl Hexyl Phthalate
Di ethyl Hexyl Phthalate
C, 5 - Terpineol
?
?
Approximate
Level
(ppb)
—
4
3
1
11
1
1
1
1
1
1

-------
                               78
                            TABLE  B136
     Organic Compounds  Identified  in  Base  Extract  of  Sample  No.  43B

Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
2.387
2.546
2.665
2.801


Compound
Camphor (IS)
Di ethyl Hexyl Phthalate
C-.C Terpineol
?
?
Approximate
Level
(ppb)
—
2
1
2
3
                            TABLE B137
       Volatile Organic Compounds  Identified in Sample No. 44S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       0.736      Dimethoxymethane                             2
  2       1.000      Chloroform                                   2
  3       2.143      Dichlorobenzene                             8
  4       2.220      Dichlorobenzene                             10

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                               79
                           TABLE B138
    Organic Compounds Identified in Acid Extract of Sample No.  44A
Peak
No.
1
2
3
4
5
7
8
9
10
11
12
13
Relative
Retention
Time
0.456
0.496
0.582
0.638
0.692
0.861
0.896
1.000
1.100
1.207
1.279
1.339
Approximate
Level
Compound (ppb)
Methyl -2-Ethyl Hexanoate (IS)
Methyl -2 ,2-Dichloro-3-Methyl Butanoate
Dichlorinated Hydrocarbon C > 5
Dichlorinated Hydrocarbon C > 5
?
Al kyl Benzene
Methyl Myri state
Methyl Palmitate
Methyl Stearate
C-,r Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
_ _ _
59
21
5
1
1
2
5
4
2
1
1
                           TABLE B139
    Organic Compounds  Identified in Base Extract of Sample No.44B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.008      Dibutyl Phthalate                            1
  3       2.463      Diethyl Hexyl Phthalate                      2
  4       2.590      C,c Terpineol                                1

-------
                           80
                       TABLE B140
   Volatile Organic Compounds  Identified  in  Sample  No.  45S
Peak
No.
1
2
3
Relative
Retention
Time
0.532
1 . 000
1.559
Compound
Acetone
Chloroform
Benzene
Approximate
Level
(ppb)
1
4
1
                       TABLE B141
Organic Compounds Identified in Acid Extract of Sample  No.  45A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.450
0.900
0.959
1.000
1.099
1.200
1.337
1.406
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Hexachloro-hexafluoropentane
Methyl Palmitate
Methyl Stearate.
C, c Terpene
Di ethyl Hexyl Phthalate
C,r - Terpineol
Approximate
Level
(ppb)
___
2
1
6
4
2
1
1

-------
                               81
                            TABLE  B142
     Organic  Compounds  Identified  in  Base  Extract of Sample No. 45B
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.991
2.384
2.566
2.691
Compound
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
C-,r Terpineol
?
Approximate
Level
(ppb)
— — —
1
2
1
1
                            TABLE B143
       Volatile Organic Compounds Identified in Sample No. 46S

       Relative                                            Approximate
Peak   Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       0.552      Acetone                                      1
  2       1.000      Chloroform                                   2
  3       1.534      Benzene                                      1
  4       2.095      Dichlorobenzene                             10

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                              82
                           TABLE B144
    Organic Compounds Identified in Acid Extract of Sample  No.  46A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.450
1.000
1.099
1.199
1.282
1.331
1.392
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,r Terpene
Wz
Diethyl Hexyl Phthalate
C, 5 - Terpineol
Approximate
Level
(ppb)
___
5
4
2
1
1
1
                           TABLE B145
    Organic Compounds  Identified in Base Extract of Sample No. 46B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.427      Diethyl Hexyl Phthalate                      1
  3       2.551      C15 Terpineol                                1
  4       2.675      ?                                            1
  5       2.831      ?                                            1

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                               83
                            TABLE B146
       Volatile Organic Compounds Identified in Sample No. 47S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

                   No peaks over 1 PPB.
                            TABLE B147
     Organic  Compounds  Identified  in Acid  Extract of Sample  No.  47A

Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.450
1.000
1.095
1.328
1.393
1.463
1.552


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C-,,- - Terpineol
?
?
Approximate
Level
(ppb)
_ _ _
3
2
1
1
1
1

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                          84
                       TABLE 6148
Organic Compounds Identified in Base  Extract  of  Sample No.47B
Peak
No.
1
2
3
4
5


Peak
No.
Relative
Retention
Time
1.000
2.399
2.516
2.643
2.797

Volatile
Relative
Retention
Time
Compound
Camphor (IS)
Diethyl Hexyl Phthalate
C,5 Terpineol
?
?
TABLE B149
Organic Compounds Identified in Sample No.
Compound
Approximate
Level
(ppb)
_ —
1
1
2
2

48S
Approximate
Level
(ppb)
No peaks over 1 PPB.


TABLE B150
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.443
1.000
1.096
1.198
1.270
1.397
Compound
Methyl -2-Ethyl Hexanoate (IS)
. Methyl Pa Imitate
Methyl Stearate
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
C, c - Terpineol

No. 48A
Approximate
Level
(ppb)
—
1
1
1
1
1

-------
                               85
                           TABLE B151
    Organic Compounds Identified in Base Extract of Sample No.48B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.593      C15 Terpineol                                1
                           TABLE B152
       Volatile Organic Compounds Identified in Sample No.  49S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.631
1.000
1.508
1.934
1.986
Compound
Freon-11
Chloroform
Trichloroethylene
Trichloropropane
Tetrachloroethylene
Approximate
Level
(ppb)
1
2
1
2
1

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                               86
                           TABLE B153
    Organic Compounds Identified in Acid Extract of Sample  No.  49A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.438
1.000
1.101
1.232
1.279
1.336
1.403
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Wz
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C15 - Terpineol
Approximate
Level
(ppb)
_ _ _
3
4
2
3
1
1
                           TABLE B154
    Organic Compounds  Identified in Base Extract of Sample No. 49B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1       1.000      Camphor (IS)
 2       2.025      Dibutyl Phthalate                            1
 3       2.478      Diethyl Hexyl Phthalate                      2

-------
                               87
                            TABLE B155
       Volatile Organic Compounds Identified in Sample No. 60S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   2
                            TABLE B156
    Organic Compounds  Identified  in Acid Extract of Sample No.  50A

Peak
No.
1
2
3
Relative
Retention
Time
0.447
1.000
1.096


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
	
2
2
                            TABLE B157
     Organic Compounds Identified in Base Extract of Sample No.508

        Relstive                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1      1.000      Camphor (IS)
  2      1.964      Dibutyl Phthalate                            1
  3      2.390      Diethyl Hexyl Phthalate                      1
  4      2.509      C15 Terpineol                                1

-------
                        88
                    TABLE B158
Volatile Organic Compounds Identified in Sample No.   51S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13

Relative
Retention
Time
0.502
0.835
1.000
1.101
1.233
1.302
1.429
1.514
1.559
1.779
1.928
2.007
2.108

Compound
Acetone
Tetrahydrofuran
Chloroform
Pentane
Carbon Tetrachloride
Bromo-Dichloromethane
?
Trichloroethylene
Di bromo-Chl oromethane
Tribromomethane
Bromobenzene
Tetrachloroethylene
Toluene
TABLE B159
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
Relative
Retention
Time
0.454
1.000
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Approximate
Level
(ppb)
3
1
47
1
2
10
4
1
6
1
38
2
1

of Sample No. 51A
Approximate
Level
(ppb)
— — -
1

-------
                          89
                       TABLE B160
Organic Compounds Identified in Base  Extract  of  Sample  No.51B
Peak
No.
1
2


Peak
No.
1
2
3

Relative
Retention
Time
1.000
2.460

Volatile
Relative
Retention
Time
1.000
1.496
1.986

Compound
Camphor (IS)
Diethyl Hexyl Phthalate
TABLE B161
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Tetrachloroethylene
TABLE B162
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.445
1.000
1 . 1 03
1.247
1.343
1.409
1.461
1.552
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Pa Imitate
Methyl Stearate
Dioctyl Adipate
Diethyl Hexyl Phthalate
C,5 - Terpineol
?
?
Approximate
Level
(ppb)
___
1

52S
Approximate
Level
(ppb)
2
2
2

No. 52A
Approximate
Level
(ppb)
— _ —
4
4
2
1
2
1
1

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                          90
                       TABLE B163
Organic Compounds Identified in Base  Extract  of  Sample No.52B
Peak
No.
1
2
3
4
5


Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Relative
Retention
Time
1.000
1.556 .
2.089
2.564
2.693

Volatile
Relative
Retention
Time
0.538
0.769
0.895
0.963
1.000
1.084
1.220
1.288
1.425
1.493
1.530
1.666
1.750
1.960
2.086
Compound
Camphor (IS)
C,0 Terpineol
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,5 - Terpineol
TABLE B164
Organic Compounds Identified in Sample No.
Compound
Acetone
Dimethoxymethane
2-Methyl Propanal
1 ,2-Dichloroethane
Chloroform
1 ,2-Dichloroethane
Carbon Tetrachloride
Bromo-Di chl oromethane
?
Trichloroethylene
Di bromo-Chl oromethane
Dichloro-Iodomethane
Tribromomethane
Dichlorobenzene
Dichlorobenzene
Approximate
Level
(ppb)
— — _
1
1
2
1

53S
Approximate
Level
(ppb)
1
8
1
4
68
4
1
12
1
1
10
1
1
10
15

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                           91
                       TABLE B165
Organic Compounds Identified in Acid Extract of Sample No.  53A
Peak
No.
1
2
3
4

Relative
Retention
Time
0.450
1.000
1.338
1.409

Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Diethyl Hexyl Phthalate
C15 - Terpineol
TABLE B166
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
4
5


Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.658
2.053
2.511
2.643

Volatile
Relative
Retention
Time
1.000
1.516
1.559
Compound
Camphor (IS)
C,Q Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
C,r Terpineol
TABLE B167
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Benzene
Approximate
Level
(ppb)
	
1
1
1

No.538
Approximate
Level
(ppb)
...
3
1
2
2

54S
Approximate
Level
(ppb)
1
2
1

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                           92
                       TABLE B168
Organic Compounds Identified in Acid Extract of Sample No.  54A
Peak
No.
1
2
3
4
5

Relative
Retention
Time
0.450
1.000
1.103
1.342
1.409

Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, 5 - Terpineol
TABLE B169
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3


Peak
No.
1
2
3
Relative
Retention
Time
1.000
2.053
2.505

Volatile
Relative
Retention
Time
1.000
1.488
1.965
Compound
Camphor (IS)
Di butyl Phthalate
Diethyl Hexyl Phthalate
TABLE B170
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Tetrachloroethylene
Approximate
Level
(ppb)
_ _ _
1
1
1
1

No. 54B
Approximate
Level
(ppb)
_ —
1
1

55S
Approximate
Level
(ppb)
2
1
1

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                               93
                           TABLE  B171
    Organic Compounds Identified in Acid Extract of Sample No. 55A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.450
1.000
1.097
1.332
1.398
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, c - Terpineol
Approximate
Level
(ppb)
_ _ _
1
2
1
1
                            TABLE B172
     Organic Compounds Identified in Base Extract  of Sample  No.  55B

Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.955
2.373


Compound
Camphor (IS)
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
1
                            TABLE B173
       Volatile Organic Compounds Identified in Sample No. 56S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   2
  2       1.531      Trichloroethylene                            1
  3       2.040      Tetrachloroethylene                          1

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                           94
                       TABLE B174
Organic Compounds Identified in Acid  Extract  of  Sample  No.56A
Peak
No.
1
2
3
4
5

Relative
Retention
Time
0.432
1.000
1.097
1.333
1.400

Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C,r - Terpineol
TABLE B175
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
4


Peak
No.
1
2
3
Relative
Retention
Time
1.000
2.048
2.506
2.637

Volatile
Relative
Retention
Time
1.000
1.493
1.966
Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,r Terpineol
TABLE B176
Organic Compounds Identified in Sample No.
Compound
Chloroform
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
_ _ _
3
2
1
1

No. 56B
Approximate
Level
(ppb)
...
2
2
2

57 S
Approximate
Level
(ppb)
1
2
2

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                           95
                       TABLE B177
Organic Compounds Identified in Acid Extract of Sample  No.  57A
Peak
No.
1
2
3
Relative
Retention
Time
0.439
1.000
1.097
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl S tea rate
Approximate
Level
(ppb)
___
5
5
                       TABLE 8178
 Organic  Compounds  Identified in Base Extract of Sample No. 578

Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.885
2.570


Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
1
1
                        TABLE  B179
   Volatile Organic Compounds Identified in Sample No.58S
Peak
No.
1
2
Relative
Retention
Time
0.499
1.000
Compound
Acetone
Chloroform
Approximate
Level
(ppb)
1
3

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                           96
                       TABLE B180
Organic Compounds Identified in Acid Extract of Sample No.  58A
Peak
No.
1
2
3
4
5
6

Relative
Retention
Time
0.415
0.890
1.000
1.098
1.137
1.404

Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C15 - Terpineol
TABLE B181
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3


Peak
No.
1
2
Relative
Retention
Time
1.000
1.807
2.442

Volatile
Relative
Retention
Time
1.000
1.937
Compound
Camphor (IS)
?
Diethyl Hexyl Phthalate
TABLE B182
Organic Compounds Identified in Sample No.
Compound
Chloroform
Bromobenzene
Approximate
Level
(ppb)
___
1
4
4
1
1

No. 58B
Approximate
Level
(ppb)
— _ —
1
2

59S
Approximate
Level
(ppb)
1
3

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                               97
                            TABLE  B183
    Organic Compounds Identified in Acid Extract of Sample No. 59A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.393
1.000
1.102
1.334
1.400
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C-,r - Terpineol
Approximate
Level
(ppb)
— _ _
4
3
2
2
                           TABLE  B184
    Organic Compounds  Identified  in Base Extract of Sample No.  59B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.047      Dibutyl Phthalate                             3
  3       2.505      Diethyl Hexyl  Phthalate                       1
  4       2.632      C.,. Terpineol                                 1
                     I 3

-------
                           98
                       TABLE B185
   Volatile Organic Compounds Identified  in Sample No.  60S
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.471
1.000
1.124
1.304
1.343
1.484
1.575
1.619
1.642
2.216
Compound
Acetone
Chloroform
Pentane
Ethyl Acetate
Bromo-Dichloromethane
Dichloropropane
Trichloroethylene
Benzene
Di bromo-Chl oromethane
Toluene
Approximate
Level
(ppb)
1
30
2
1
5
1
1
1
1
2
                       TABLE B186
Organic Compounds Identified in Acid Extract of Sample No.  60A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.442
1.000
1.103
1.343


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
4
3
1

-------
                               99
                            TABLE B187

     Organic Compounds Identified in Base Extract of Sample No.60B


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1      1.000      Camphor (IS)

  2      1.517      C]0 Terpineol                                1
  3      2.477      Diethyl Hexyl Phthalate                      1
                            TABLE  B188
       Volatile Organic Compounds Identified in Sample No. 61S


       Relative                                            Approximate
Peak   Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                    1
  2       1.519      Trichloroethylene                             1

  3       1.696      Hexane                                        1

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                           100
                       TABLE B189
Organic Compounds Identified in Acid Extract of Sample No.  61A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.450
1.000
1.097
1.266
1.278
1.308
1.339
1.360
1.387
1.442
1.481
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Methyl Dihydroabietate
Fatty Acid Methyl Ester C >_ 22
Hydrocarbon C > 26
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C _> 24
Hydrocarbon C > 28
Fatty Acid Methyl Ester C >_ 26
Hydrocarbon C > 8
Approximate
Level
(ppb)
_ _ _
4
4
3
3
2
2
5
3
8
4

-------
                          101
                       TABLE  B190
Organic Compounds Identified  in  Base  Extract  of Sample No.61B
Peak
No.
1
2
3
4
5
6
7
8
9


Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
1.000
1.903
2.059
2.203
2.266
2.537
2.583
2.594
2.669

Volatile
Relative
Retention
Time
0.864
1.000
1.082
1.187
1.537
1.936
2.007
2.045
Compound
Camphor (IS)
Anthracene
Di butyl Phthalate
C16H10
C16H10
Diethyl Hexyl Phthalate
C18H12
C18H12
C,r Terpineol
TABLE B191
Organic Compounds Identified in Sample No.
Compound /
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Bromo-Dichloromethane
Trichloroethylene
4-Methyl-2-Ethyl-l ,3-Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrach 1 oroethyl ene
Approximate
Level
(ppb)
___
1
1
2
3
2
1
1
1

62S
Approximate
Level
(ppb)
3
4
10
2
2
1
1
2

-------
                           102
                       TABLE B192
Organic Compounds Identified in Acid  Extract  of  Sample No.62A
Peak
No.
1
2
3
5
6
7
8
9
10

Relative
Retention
Time
0.442
0.894
0.948
1.000
1.070
1.206
1.282
1.343
1.412

Approximate
Level
Compound (ppb)
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Fatty Acid Methyl Ester C >_ 15
Methyl Palmitate
C,r Terpene
C,r Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
C,g - Terpineol
TABLE B193
Organic Compounds Identified in Base Extract of Sample
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
2.018
2.059
2.365
2.477
2.606
Compound
Camphor (IS)
Di butyl Phthalate
Dibutyl Nonanedioate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Clf- Terpineol
— — —
6
2
16
2
7
6
2
1

No.626
Approximate
Level
(ppb)
— __
2
2
3
2
1

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                        103
                    TABLE B194
Volatile Organic Compounds  Identified  in  Sample  No.  63S
Peak
No.
1
2
3
4
5
6
7
8

Relative
Retention
Time
0.872
1.000
1.075
1.368
1.506
1.895
1.970
2.007

Compound
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Bromo-Di chl oroethane
Trichloroethylene
Ethyl Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
TABLE B195
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.431
0.890
0.945
1.000
1.091
1.128
1.164
1.177
1.204
1.225
1.277
1.341
1.362
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Palmitate
Methyl Stearate
?
C, 5 Terpene
Diisobutyl Phthalate
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
Approximate
Level
(ppb)
2
6
9
9
3
1
1
2

Sample No. 63A
Approximate
Level
(ppb)
_ —
6
1
19
13
3
3
3
3
2
23
3
1

-------
                          104
                       TABLE  B196
Organic Compounds Identified  in Base  Extract  of  Sample  No.  63B
Peak
No.
1
2
3
4
5
6


Peak
No.
1
2
.3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.260
1.555
2.066
2.424
2.540

Volatile
Relative
Retention
Time
0.882
1.000
1.081
1.366
1.512
1.840
1.910
1.986
2.020
Compound
Camphor (IS)
Benzothiazole
C n Terpineol
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
TABLE B197
Organic Compounds Identified in Sample No.
Compound
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
Bromo-Dichl oroethane
Trichloroethylene
?
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
— -
6
1
1
4
2

64S
Approximate
Level
(ppb)
4
10
8
1
4
1
1
1
2

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                               105
                           TABLE B198
    Organic Compounds  Identified  in  Acid  Extract  of  Sample  No.  64A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.416
0.887
1.000
1.091
1.198
1.219
1.271
1.341
1.411
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myrsitate
Methyl Palmitate
Methyl Stearate
C Terpene
?
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C, 5 - Terpineol
Approximate
Level
(ppb)
—
2
6
4
3
1
1
2
1
                           TABLE B199
    Organic Compounds  Identified in Base Extract of Sample No. 64B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       1.286      Benzothiazole                                2
  3       1.549      C,Q Terpineol                                1
  4       2.053      Dibutyl Phthalate                            1
  5       2.523      Diethyl Hexyl Phthalate                      1
  6       2.654      C,5 Terpineol                                1

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                        106
                    TABLE B200
Volatile Organic Compounds Identified in Sample No.  65S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15

Relative
Retention
Time
0.456
0.876
0.957
1.000
1.086
1.193
1.382
1.431
1.522
1.678
1.792
1.846
1.921
1.991
2.028

Compound
Dichloromethane
Tetrahydrofuran
1 ,2-Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Bromo-Chloroethane
1 ,2-Dichloropropane
Trichloroethylene
1 -Bromo-2-Chl oropropane
Tribromomethane
?
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
TABLE B201'
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.434
1.000
1.097
1.228
1.280
1.341
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
?
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
15
3
20
9
2
1
1
8
2
2
2
8
3
6

Sample No. 65A
Approximate
Level
(ppb)
_ _ _
3
3
1
1
2

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                          107
                       TABLE B202
Organic Compounds Identified in Base Extract of Sample  No.  65B
Peak
No.
1
2
3
4
5
6
7
8


Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
1.000
1.177
1.544
1.595
1.744
1.876
2.047
2.511

Volatile
Relative
Retention
Time
0.451
0.877
0.957
1.000
1.085
1.186
1.506
1.655
1.773
1.826
1.895
1.970
2.007
Compound
Camphor (IS)
Bromopropyl Benzene
C22H14
?
C,n Camphenol
C,Q Camphenol
Dibutyl Phthalate
Di ethyl Hexyl Phthalate
TABLE B203
Organic Compounds Identified in Sample No.
Compound
Dichloromethane
Tetrahydrofuran
1 ,2-Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 -Chi oro-2-Bromopropane
Tribromomethane
?
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
Approximate
Level
(ppb)
_ — —
3
2
3
2
2
1
1

66S
Approximate
Level
(ppb)
2
15
2
14
9
1
8
1
1
1
12
2
6

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                          108
                       TABLE B204
Organic Compounds Identified in Acid Extract of Sample No.  66A
Peak
No.
1
2
.3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
Relative
Retention
Time
0.429
0.670
0.890
0.900
0.920
0.948
0.969
1.000
1.009
1.058
1.101
1.207
1.231
1.281
1.345
1.369
1.415
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloroanisole
Methyl Myri state
Methyl Dichlorophenoxy Acetate
Methyl Dichlorophenoxy Acetate
Pentachloroanisole
Methyl -2 (4-chlorophenoxy)Butanoate
Methyl Palmitate
Cnr Terpene
?
Methyl Stearate
C, 5 Terpene
?
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
?
C,c - Terpineol
Approximate
Level
(ppb)
_ — _
1
3
1
1
1
2
8
2
2
5
3
3
19
2
2
2
                        TABLE B205
 Organic Compounds Identified in Base Extract of Sample No.  66B
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.552
1.604
2.069
2.424
2.540
Compound
Camphor (IS)
C5H10C12
?
Di butyl Phthalate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
2
1
2
10
1

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                        109
                    TABLE B206
Volatile Organic Compounds Identified  in  Sample  No. 67S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11

Relative
Retention
Time
0.459
0.882
1.000
1.075
1.182
1.509
1.662
1.777
1.991
1.986
2.018

Compound
Dichloromethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 -Chi oro-2-Bromoethane
Tribromomethane
Ethyl -Methyl Dioxolane
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
TABLE B207
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.440
0.897
0.953
1.000
1.051
1.097
1.328
1.393
1.460
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Palmitate
?
Methyl Stearate
Diethyl Hexyl Phthalate
C,5 Terpineol
?
Approximate
Level
(ppb)
2
5
6
8
1
8
3
1
4
6
9

Sample No. 67A
Approximate
Level
(ppb)
—
1
1
10
1
10
2
1
1

-------
                          no
                      TABLE B208
Organic Compounds  Identified in Base Extract of Sample  No.67B
Peak
No.
1
2
3
4
5


Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
1.000
2.562
2.688
2.821
2.975

Volatile
Relative
Retention
Time
0.439
0.881
0.951
1.000
1.035
1.183
1.512
1.975
2.002
2.056
2.179
Compound
Camphor (IS)
Diethyl Hexyl Phthalate
C-|5 Terpineol
?
?
TABU B^oy
Organic Compounds Identified in Sample No.
Compound
Dichloromethane
Tetrahydrofuran
1,2-Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1,1-Trichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
Dichlorobenzene
Dichlorobenzene
Approximate
Level
(ppb)
___
2
1
1
1

68S
Approximate
Level
(ppb)
2
1
2
4
1
1
4
1
4
8
8

-------
                               Ill
                           TABLE B210
    Organic Compounds Identified in Acid Extract of Sample No.  68A
Peak
No.
1
2
3
4
5
5
6
Relative
Retention
Time
0.422
0.800
0.867
1.000
1.027
1.068
1.301
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
Methyl Myri state
Methyl Palmitate
?
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
1
2
6
1
5
3
                           TABLE B211
    Organic Compounds  Identified in Base Extract of Sample No. 68B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       1.646      Unidentified Phthalate                        1
  3       2.024      Dibutyl  Phthalate                             1
  4       2.439      Diethyl  Hexyl Phthalate                       1
  5       2.576      C 5 Terpineol                                 1
  6       2.713      ?                                             1
  7       2.861      ?                                             2

-------
                        112
                    TABLE B212
Volatile Organic Compounds Identified  in  Sample  No.  69S
Peak
No.
1
2
3
4
5
6
7
8

Relative
Retention
Time
0.442
0.881
1.000
1.081
1.184
1.509
1.975
2.013

Compound
Dichloromethane
Tetrahydrofuran
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachloroethylene
TABLE B213
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.450
0.800
0.900
1.000
1.062
1.102
1.204
1.264
1.279
1.339
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
Methyl Myri state
Methyl Palmitate
Hydrocarbon C > 18
Methyl Stearate
C,5 Terpene
Hydrocarbon C > 24
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
12
3
3
10
9
8

Sample No. 69A
Approximate
Level
(ppb)
—
2
4
11
2
9
3
2
2
2

-------
                               113
                           TABLE B214

    Organic Compounds Identified in Base Extract of Sample No. 69B
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
2.027
2.463
2.593
2.675
2.720
2.897
Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,5 Terpineol
Hydrocarbon C ^ 30
?
?
Approximate
Level
(ppb)
___
1
1
1
1
2
2
                            TABLE B215
       Volatile Organic Compounds Identified in Sample No. 70S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   2
  2       1.080      1,2-Dichloroethane                           2

  3       1.514      Trichloroethylene                            2

  4       2.018      Tetrachloroethylene                          4

-------
                           114
                       TABLE B216
Organic Compounds Identified in Acid Extract of Sample  No.  70A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.445
0.533
0.895
0.952
1.000
1.036
1.054
1.105
1.129
1.207
1.219
1.228
1.249
1.270
1.285
1.355
1.432
1.456
1.526
1.559
Compound
Methyl -2-Ethyl Hexanoate (IS)
Hexachlorobutadiene
Methyl Myri state
Pentachloroanisole
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
Fatty Acid Methyl Ester C 1 16
Methyl Stearate
?
C,r Terpene
?
Hydrocarbon C >_ 22
Dioctyl Adi pate
Hydrocarbon C > 22
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Hydrocarbon C > 26
?
Hydrocarbon C > 28
Hydrocarbon C >• 30
Approximate
Level
(ppb)
V — _
1
9
2
28
5
7
29
17
7
7
9
20
9
12
1264
13
43
14
21

-------
                          115
                       TABLE B217
Organic Compounds Identified in Base  Extract  of Sample  No.  70B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
Relative
Retention
Time
0.803
1.000
1.028
1.517
1.539
1.630
1.730
1.786
1.865
1.910
1.938
2.051
2.118
2.160
2.200
2.260
2.290
2.326
2.360
2.398
2.472
2.635
2.685
2.730
2.815
2.854
2.882
2.921
Compound
Hexachloroethane
Camphor (IS)
Hexachlorobutadiene
Hydrocarbon C >_ 14
Hydrocarbon C ^ 14
Hydrocarbon C >_ 16
Hydrocarbon C >_ 16
Hydrocarbon C >_ 18
Hydrocarbon C >_ 18
Hydrocarbon C >_ 18
Hydrocarbon C > 18
Di butyl Phthalate
Hydrocarbon C >_ 20
Unidentified Phthalate
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
Dioctyl Adi pate
Hydrocarbon C >_ 22
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Hydrocarbon C ^ 30
?
Hydrocarbon C ^ 30
Unidentified Phthalate
Hydrocarbon C >_ 30
Hydrocarbon C ^ 30
?
Approximate
Level
(ppb)
1
—
1
9
13
12
11
6
11
8
16
14
21
4
8
4
4
14
3
14
2347
13
65
200
7
34
13
92

-------
                       116
                    TABLE B218
Volatile Organic Compounds Identified  in  Sample  No. 71S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.067.
1.444
1.893
1.924
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
2
2
3
1
3

-------
                           117
                       TABLE B219
Organic Compounds Identified in Acid Extract of Sample  No.  71A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.428
0.778
0.820
0.892
0.931
0.946
1.000
1.039
1.051
1.096
1.201
1.245
1.275
1.305
1.335
1.356
1.374
1.400
1.476
1.559
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
C,Q Terpineol
Methyl Myri state
Fatty Acid Methyl Ester C i 14
Pentachloroanisole
Methyl Palmitate
Unidentified Phthalate
Fatty Acid Methyl Ester C 1 16
Methyl Stearate
C.c Terpene
1 b
Dioctyl Adi pate
Butyl Phthalyl Butyl Glycolate
Butyl Benzyl Phthalate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 22
Dioctyl Phthalate
C,,- Terpineol
?
?
Approximate
Level
(ppb)
___
2
2
3
1
1
9
1
1
11
1
2
2
1
2
2
2
3
2
6

-------
                          118
                       TABLE B220
Organic Compounds Identified in Base  Extract of Sample No.  71B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
Relative
Retention
Time
1.000
1.508
1.610
1.708
1.805
1.903
2.000
2.038
2.060
2.069
2.157
2.238
2.270
2.314
2.335
2.384
2.438
2.459
2.508
2.529
2.562
2.600
2.638
2.670
2.692
2.746
2.784
2.843
Compound
Camphor (IS)
C,Q Terpineol
Hydrocarbon C >_ 14
Hydrocarbon C >_ 16
Hydrocarbon C ^ 16
Diisobutyl Phthalate
Dibutyl Phthalate
Diisobutyl Nonanedioate
?
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
Hydrocarbon C >_ 22
Dioctyl Adi pate
Hydrocarbon C >_ 22
?
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Hydrocarbon C >_ 24
Dicyclohexyl Phthalate
Hydrocarbon C >_ 26
C-.C- Terpineol
Hydrocarbon C ^ 26
?
Hydrocarbon C >_ 28
?
Hydrocarbon C >_ 28
Hydrocarbon C >_ 28
?
Approximate
Level
(ppb)
___
3
3
3
3
9
20
4
8
5
6
9
10
5
4
15
19
5
7
5
12
5
6
4
8
7
7
20

-------
                          119
                       TABLE B221
   Volatile Organic Compounds  Identified  in  Sample  No.  72S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.081
1.514
1.986
2.018
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
2
2
2
1
2
                       TABLE B222
Organic Compounds Identified in Acid Extract of Sample  No.  72A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.437
0.882
0.895
1.000
1.099
1.277
1.337
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
1
2
3
1
1

-------
                               120
                            TABLE  B223
     Organic Compounds  Identified  in  Base  Extract of Sample No.  72B
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.525
2.034
2.374
2.486
2.620
Compound
Camphor (IS)
C,Q - Terpineol
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
C-|5 Terpineol
Approximate
Level
(ppb)
- _ _
1
3
3
33
3
                            TABLE  B224

       Volatile Organic Compounds Identified in Sample No. 73S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   2

  2       1.075      1,2-Dichloroethane                           1

  3       1.504      Trichloroethylene                            1

  4       2.007      Tetrachloroethylene                          1

-------
                               121
                           TABLE B225
    Organic Compounds Identified in Acid Extract  of Sample  No.  73A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.433
0.780
0.819
0.894
1.000
1.096
1.338
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
C, Q Terpineol
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— __
3
6
2
7
5
1
                           TABLE B226
    Organic Compounds  Identified in Base Extract of Sample No. 73B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       1.517      C]0 Terpineol                                1
  3       2.018      Dibutyl Phthalate                            1
  4       2.463      Diethyl Hexyl Phthalate                      1

-------
                           122
                       TABLE B227
   Volatile Organic Compounds  Identified  in  Sample  No.  74S
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.080
1.996
Compound
Chloroform
1 ,2-Dichloroethane
Tetrachloroethylene
Approximate
Level
(ppb)
2
2
1
                       TABLE B228
Organic Compounds Identified in Acid Extract of Sample  No.  74A

Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.435
0.813
1.000
1.098
1.330
1.402


Compound
Methyl -2-Ethyl Hexanoate (IS)
C, 0 Terpineol
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C,r Terpineol
Approximate
Level
(ppb)
___
3
4
3
5
1

-------
                               123
                           TABLE B229
    Organic Compounds Identified in Base Extract of Sample No. 74B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       1.511      CIQ Terpineol                                2
                           TABLE B230
       Volatile Organic Compounds Identified in Sample No.   75S

Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.095
1.330
1.615
2.009
2.103
2.259


Compound
Chloroform
1 ,2-Dichloroethane
Bromo-Dichloromethane
Di bromo-Chl oromethane
Dichlorobenzene
Toluene
Dichlorobenzene
Approximate
Level
(ppb)
22
2
4
1
1
1
1

-------
                               124
                           TABLE B231
    Organic Compounds Identified in Acid Extract of Sample  No.  75A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.440
0.816
1.000
1.039
1.103
1.139
1.184
1.226
1.269
1.281
1.311
1.341
1.389
1.407
Compound
Methyl -2-Ethyl Hexanoate (IS)
C-.Q Terpineol
Methyl Palmitate
Hydrocarbon C > 18
Methyl Stearate
Hydrocarbon C > 20
Hydrocarbon C > 20
Hydrocarbon C > 22
Hydrocarbon C > 22
Butyl Phthalyl Butyl Glycolate
Hydrocarbon C > 24
Di ethyl Hexyl Phthalate
Hydrocarbon C >_ 26
C, [- Terpineol
Approximate
Level
(ppb)
__ —
2
6
1
4
1
1
1
1
1
1
1
1
1
                           TABLE B232
    Organic Compounds  Identified in Base Extract of Sample No. 75B

       Relative                                            Approximate
Peak  Retention                                            .   Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       1.521      C,Q Terpineol                                2
  3       2.000      Dibutyl  Phthalate                            1
  4       2.486      Diethyl  Hexyl Phthalate                      1

-------
                               125
                            TABLE B233

       Volatile Organic Compounds Identified in Sample No. 76S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   1

  2       1.554      Trichloroethylene                            1
                            TABLE B234

     Organic  Compounds  Identified  in Acid Extract of Sample No.  76A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.440
0.817
0.898
1.000
1.099
1.347
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— •. —
2
1
3
3
3

-------
                               126
                           TABLE B235

    Organic Compounds  Identified in Base Extract of Sample No. 76B
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.521
2.020
2.459
2.620
2.711
2.859
Compound
Camphor (IS)
C,n - Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
C,5 - Terpineol
?
?
Approximate
Level
(ppb)
_ — _
4
1
1
1
2
2
                            TABLE  B236
       Volatile Organic Compounds Identified in Sample No. 77S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                  15

  2       1.562      Trichloroethylene                            1

-------
                               127
                           TABLE B237
    Organic Compounds Identified in Acid Extract of Sample No.  77A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.432
0.780
0.893
1.000
1.098
1.333
1.399
1.467
1.535
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, ,- Terpineol
?
?
Approximate
Level
(ppb)
___
2
2
4
3
1
1
1
1
                           TABLE B238
    Organic Compounds  Identified in Base Extract of Sample No. 77B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       1.543      C,Q - Terpineol                              1
  3       2.054      Dibutyl Phthalate                            1
  4       2.508      Diethyl Hexyl Phthalate                      1
  5       2.766      ?                                            1
  6       2.900      ?                                            2

-------
                          128
                       TABLE B239
   Volatile  Organic  Compounds  Identified  in  Sample No.  78S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.076
1.519
1.959
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachloroethylene
Approximate
Level
(ppb)
10
5
3
2
                       TABLE B240
Organic Compounds Identified in Acid Extract of Sample  No.  78A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.412
1.000
1.103
1.339
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
...
2
2
1
                       TABLE B241
Organic Compounds Identified in Base Extract of Sample No. 78B

Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.548
2.062
2.508


Compound
Camphor (IS)
C,Q - Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
1
1

-------
                               129
                            TABLE  B242
       Volatile Organic Compounds Identified in Sample No. 79S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1      1.000      Chloroform                                   1

  2      1.975      Dichlorobenzene                              3
                            TABLE B243

     Organic  Compounds  Identified  in Acid  Extract of Sample No.  79A

Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.435
0.816
1.000
1.098
1.321


Compound
Methyl -2-Ethyl Hexanoate (IS)
C, Q Terpineol
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
1
2
2
1
                            TABLE B244

     Organic Compounds Identified in Base Extract of Sample No.  79B

Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.516
2.027
2.457


Compound
Camphor (IS)
C,Q - Terpineol
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
3
1
1

-------
                               130
                            TABLE  B245

       Volatile Organic Compounds Identified in Sample No.  80S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1      1.000      Chloroform                                   2
                            TABLE B246
    Organic Compounds  Identified  in Acid Extract of Sample No. 80A
Peak
No.
1
2
.3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.435
0.818
0.869
0.922
0.976
1.000
1.027
1.078
1.093
1.164
1.206
1.248
1.343
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
C-.,- Alcohol
C,c Alcohol
1 b
C,y Alcohol
Methyl Palmitate
C,g Alcohol
C,g Alcohol
Methyl Stearate
C2Q Alcohol
C_, Alcohol
C22 Alcohol
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
4
4
3
1
5
1
1
3
1
1
1
1

-------
                               131
                           TABLE B247
    Organic Compounds Identified in Base Extract of Sample No. SOB

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.667      Diethyl Hexyl Phthalate                      1
  3       2.800      C]5 - Terpineol                              1
  4       2.981      ?                                            1
  5       3.095      ?                                            1
                            TABLE B248
       Volatile Organic Compounds  Identified in Sample No. 81S

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time      Compound                                   (ppb)

  1       1.000     Chloroform                                   14
  2       1.528     Trichloroethylene                             2

-------
                              132
                           TABLE B249
    Organic Compounds Identified in Acid Extract of Sample No.  81A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.450
1.000
1.098
1.260
1.328
1.396
1.461
1.541
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Methyl Dehydroabietate
Di ethyl Hexyl Phthalate
C, (- Terpineol
1 0
?
?
Approximate
Level
(ppb)
_ _ _
4
3
1
1
1
1
1
                           TABLE B250
    Organic Compounds Identified in Base Extract of Sample No. 81B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.508      Diethyl Hexyl Phthalate                      1
  3       2.635      C15 ~ TerPineo1                              1
  4       2.773      ?                                            4
  5       2.945      ?                                            3

-------
                               133
                            TABLE B251
       Volatile Organic Compounds Identified in Sample No. 82S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1      1.000      Chloroform                                  12
                            TABLE B252
     Organic Compounds Identified in Acid Extract of Sample No.   82A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.345
1.000
1.101
1.348


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
2
4
                            TABLE B253
     Organic Compounds Identified in Base Extract of Sample No. 82B

        Relative                                            Approximate
 Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)

  1      1.000      Camphor (IS)
  2      1.565      CIQ - Terpineol                              1
  3      2.102      Dibutyl Phthalate                            1
  4      2.579      Diethyl Hexyl Phthalate                      1

-------
                               134
                            TABLE B254
       Volatile Organic Compounds Identified in Sample No. 83S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   2
  2       1.500      Trichloroethylene                            2
                            TABLE B255
     Organic Compounds Identified in Acid Extract of Sample No.  83A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.424
0.819
0.890
1.000
1.104
1.347
1.415
Compound
Methyl -2-Ethyl Hexanoate (IS)
CIQ Terpineol
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C15 Terpineol
Approximate
Level
(ppb)
—
2
1
5
4
1
1

-------
                               135
                           TABLE B256
    Organic Compounds Identified in Base Extract of Sample No. 83B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       2.528      Diethyl Hexyl Phthalate                      1
                           TABLE B257
       Volatile Organic Compounds Identified in Sample No.  84S
Peak
No.
1
2
Relative
Retention
Time
1.000
1.498
Compound
Chloroform
Trichloroethylene
Approximate
Level
(Ppb)
1
1
                           TABLE B258
     Organic  Compounds  Identified in Acid Extract of Sample No. 84A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.430
1.000
1.105
1.354


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
2
1

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                              136
                           TABLE B259
    Organic Compounds Identified in Base Extract of Sample No. 84B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

                   No peaks over 1 PPB.
                           TABLE B260
       Volatile Organic Compounds Identified in Sample No.  85S
Peak
No.
1
2
.3
4
5
6
7
Relative
Retention
Time
0.958
1.000
1.078
1.182
1.506
1.980
2.017
Compound
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
1
2
1
1
3
1
3

-------
                              137
                           TABLE B261
    Organic Compounds Identified in Acid Extract of Sample No.  85A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.400
1.000
1.100
1.347
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
4
5
2
                           TABLE B262
     Organic Compounds  Identified in Base Extract of Sample No. 85B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor (IS)
  2       1.558      C]0 - Terpineol                              2
  3       2.024      Diphenyl Benzene                             1
  4       2.070      Dibutyl Phthalate                            1
  5       2.536      Diethyl Hexyl Phthalate                      2

-------
                        138
                    TABLE B263
Volatile Organic Compounds Identified in Sample  No.  86S
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.431
0.879
0.953
1.000
1.079
1.184
1.511
1.991
2.028
Compound
Dichloromethane
Tetrahydrofuran
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
1,1,1 -Tr i chl oroethane
Trichloroethylene
1 ,1 ,2,2-Tetrachloroethane
Tetrachl oroethyl ene
Approximate
Level
(ppb)
1
1
1
10
1
1
5
3
12

-------
                          139
                       TABLE B264
Organic Compounds Identified in Acid Extract  of Sample  No. 86A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time
0.419
0.666
0.766
0.888
0.899
0.927
0.967
1.000
1.061
1.103
1.139
1.207
1.234
1.271
1.350
1.416
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloroanisole
Methyl Laurate
Methyl Myri state
Methyl Dichlorophenoxy Acetate
Methyl Dichlorophenoxy Acetate
Methyl -Trichlorophenoxy Acetate
Methyl Palmitate
?
Methyl Stearate
Diphenyl Sulfone
C16H10
?
Methyl Dehydroabietate
Di ethyl Hexyl Phthalate
C, 5 Terpineol
Approximate
Level
(ppb)
_ _ _
1
1
5
6
5
5
10
2
11
4
8
6
5
24
1

-------
                          140
                       TABLE  B265
Organic Compounds Identified  in  Base  Extract of Sample No. 86B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11


Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.574
1.734
2.013
2.119
2.208
2.552
2.611
2.741
2.877
3.049

Volatile
Relative
Retentioa
Time
1.000
1.084
1.511
2.027
Compound
Camphor (IS)
C,0 - Terpineol
Diethyl Phthalate
Diisobutyl Phthalate
Di butyl Phthalate
?
Unidentified Phthalate
Diethyl Hexyl Phthalate
C,5 - Terpineol
?
?
TABLE B266
Organic Compounds Identified in Sample No.
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachloroethylene
Approximate
Level
(ppb)
_ _ _
4
5
4
5
2
1
15
1
2
5

87S
Approximate
Level
(ppb)
4
1
1
1

-------
                               141
                           TABLE B267
    Organic Compounds  Identified in Acid Extract of Sample No.  87A
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
0.425
0.765
0.814
0.887
0.945
1.000
1.104
1.351
1.421
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Laurate
C, 0 Terpineol
Methyl Myri state
Pentachloroanisole
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C15 Terpineol
Approximate
Level
(ppb)
___
1
2
1
1
8
8
1
1
                           TABLE B268
     Organic Compounds  Identified in Base Extract of Sample No. 87B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       2.071      Dibutyl  Phthalate                            1
  3       2.562      Diethyl  Hexyl Phthalate                     10
  4       2.828      ?                                            2
  5       2.990      ?                                            2

-------
                          142
                      TABLE B269
  Volatile Organic Compounds Identified in Sample No.  88S
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.456
0.954
1.000
1.483
1.777
1.970
Compound
Dichloromethane
Dichloroethylene
Chloroform
Trichloroethylene
Bromobenzene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
1
1
8
10
7
2
                       TABLE B270
Organic Compounds Identified in Acid Extract  of Sample  No. 88A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.425
1.000
1.099
1.268
1.341
1.410
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Methyl Dehydroabietate
Di ethyl Hexyl Phthalate
C, 5 Terpineol
Approximate
Level
(ppb)
___
2
1
4
1
1

-------
                               143
                           TABLE B271
     Organic Compounds  Identified in  Base  Extract of Sample No.
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
2.539
2.636
2.676
Compound
Camphor (IS)
Diethyl Hexyl Phthalate
Hydrocarbon C >_ 26
C,r - Terpineol
Approximate
Level
(ppb)
— — —
1
2
2
                            TABLE B272
       Volatile Organic Compounds Identified in Sample No. 89S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       0.927      Dichloroethylene                             1
  2       1.000      Chloroform                                   4
  3       1.084      1,2-Dichloroethane                           1
  4       1.138      Pentane                                      1
  5       1.222      Cyclohexane                                  1
  6       1.576      Trichloroethylene                            1
  7       2.128      Tetrachloroethylene                          1
  8       2.382      Dichlorobenzene                             12

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                              144
                           TABLE B273

    Organic Compounds Identified in Acid Extract of Sample No.  89A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.408
0.851
0.888
1.000
1.103
1.348
1.417
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
C, 5 Terpineol
Approximate
Level
(ppb)
___
1
1
3
2
1
1
                           TABLE B274

    Organic Compounds  Identified in Base Extract of Sample No.89B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


  1       1.000      Camphor (IS)

  2       2.639      Diethyl Hexyl Phthalate                      1

-------
                                145
                             TABLE  B275
        Volatile Organic Compounds  Identified  in  Sample  No.90S
Peak
No.
1
2
Relative
Retention
Time
1.000
1.136
Compound
Chloroform
Pentane
Approximate
Level
(ppb)
1
1
                             TABLE B276
     Organic  Compounds  Identified  in Acid Extract of Sample No.90A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.402
1.000
1.108
1.354
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
5
3
1
                             TABLE B277
    Organic Compounds Identified  in Base Extract of Sample No.90B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       2.125      Dibutyl  Phthalate                            3
  3       2.617      Diethyl  Hexyl  Phthalate                      2
  4       2.253      C]5 - Terpineol                              2

-------
                               146
                            TABLE B278
       Volatile Organic Compounds Identified in Sample No. 91S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   1
  2       1.195      Cyclohexane                                  1
  3       1.663      Hexane                                       1
                            TABLE  B279
     Organic  Compounds  Identified in Acid Extract of Sample No. 91A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.361
1.000
1.012
1.106
1.119
1.213
1.353
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
C,5 Terpene
Methyl Stearate
C,c Terpene
C,5 Terpene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
__ _
5
2
8
2
1
1

-------
                                147
                             TABLE  B280

    Organic Compounds Identified in Base Extract of Sample No. 91B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Camphor  (IS)
  2       2.594      Diethyl  Hexyl Phthalate                       1

  3       2.728      C]5  -  Terpineol                               2
                             TABLE B281

        Volatile Organic Compounds Identified in Sample No. 92S


       Relative                                             Approximate
 Peak   Retention                                               Level
 No.     Time       Compound                                   (ppb)


  1      1.000       Chloroform                                  31

  2      1.214       Cyclohexane                                  2
  3      1.573       Trichloroethylene                            1

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                           148
                        TABLE B282
Organic Compounds Identified in  Acid  Extract  of Sample No. 92A
Peak
No.
1
2
3
4
5

Relative
Retention
Time
0.400
1.000
1.102
1.121
1.210

Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
C,r Terpene
TABLE B283
Organic Compounds Identified in Base Extract
Peak
No.
1
2
3
4



Relative
Retention
Time
1.000
2.111
2.595
2.734


Volatile
Relative
Peak Retention
. No. Time
1
1.212
Compound
Camphor (IS)
Di butyl Phthalate
Di ethyl Hexyl Phthalate
C,r - Terpineol
/
TABLE B284
Organic Compounds Identified in
Compound
Cyclohexane
Approximate
Level
(ppb)
—
4
2
2
1

of Sample No. 92B
Approximate
Level
(ppb)
—
1
1
1


Sample No. 93S
Approximate
Level
(ppb)
1

-------
                               149
                            TABLE B285

    Organic Compounds Identified in Acid Extract of Sample No. 93A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.399
0.888
1.000
1.015
1.104
1.121
1.212
1.348
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
C,,- Terpene
Methyl Stearate
C,r Terpene
C,r Terpene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
2
8
1
2
3
4
1
                             TABLE  B286
    Organic Compounds Identified in Base Extract of Sample No.93B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)
1
2
3
4
5
6
1.000
1.294
1.413
1.531
.2.527
2.651
Camphor (IS) —
C,,- Hydrocarbon 1
C g Hydrocarbon 1
C,7 Hydrocarbon 1
Diethyl Hexyl Phthalate 1
C15 - Terpineol 1

-------
                           150
                        TABLE B'287
   Volatile Organic Compounds Identified in Sample No. 94S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.211
1.349
2.007
Compound
Chloroform
Cyclohexane
Bromo-Dichl
Toluene


+ 1 ,1 ,1-Trichloroethane
oromethane

Approximate
Level
(ppb)
30
1
3
1
                        TABLE B288
Organic Compounds Identified in Acid Extract of Sample No. 94A
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.229
0.341
0.400
0.416
0.498
0.688
0.752
0.816
1.000
1.351
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
Dichlorobutane
Trichloropentane
C,,- Hydrocarbon
C,g Hydrocarbon
C,7 Hydrocarbon
Methyl Palmitate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
3
1
—
1
1
1
1
1
1
1

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                                151
                             TABLE  B289

    Organic Compounds Identified in Base Extract of Sample No. 94B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


  1       1.000      Camphor  (IS)

  2       1.429      C,g Hydrocarbon                              1

  3       1.544      C,7 Hydrocarbon                              1
  4       2.550      Diethyl  Hexyl Phthalate                      1
  5       2.649      C,5 Terpineol                                1
                             TABLE  B290
        Volatile Organic Compounds  Identified  in  Sample  No.95S


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1      1.211        Cyclohexane + 1,1,1-Trichloroethane           1

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                           152
                        TABLE B291
Organic Compounds Identified in Acid Extract of Sample No.95A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.221
0.340
0.421
0.689
0.755
0.814
0.880
1.000
1.009
1.102
1.116
1.206
1.281
1 . 340
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
C-,r Hydrocarbon
C,g Hydrocarbon
C,7 Hydrocarbon
Methyl Myri state
Methyl Palmitate
C,5 Terpene
Methyl Stearate
C,5 Terpene
C,r Terpene
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
1
—
1
1
1
1
6
2
2
5
4
2
1

-------
                               153
                            TABLE B292
    Organic Compounds  Identified  in Base Extract of Sample No.95B
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.531
2.056
2.405
.2.515
2.642
Compound
Camphor (IS)
C,7 Hydrocarbon
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
C,5 - Terpineol
Approximate
Level
(ppb)
— _ —
1
1
1
2
1
                            TABLE B293
       Volatile Organic Compounds Identified in Sample No. 96S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1     1.000       Chloroform                                   1
 2     1.211       Cyclohexane + 1,1,1-Trichloroethane          1
 3     1.567       Trichloroethylene                           13
 4     2.005       Toluene                                      1

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                                154
                            TABLE  B294

    Organic Compounds  Identified in Acid Extract of Sample No. 96A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.433
1.000
1.102
1.343
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
2
2
1
                             TABLE  B295
    Organic Compounds Identified in Base Extract of Sample No.96B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)
                       No  peaks  over  1  PPB.
                             TABLE  B296

        Volatile Organic  Compounds  Identified  in  Sample  No. 97S


       Relative                                            Approximate
Peak   Retention                                              Level
 No.      Time       Compound                                   (ppb)


  1      1.181        Cyclohexane                                   1

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                               155
                            TABLE B297
    Organic Compounds Identified in Acid Extract of Sample No.  97A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.361
1.000
1.106
1.120
1.212
1.285
1.350
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
C,r Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
2
1
1
1
1
1
                             TABLE B298
    Organic Compounds  Identified  in Base Extract of Sample No.97B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       2.125      Dibutyl  Phthalate                             2
  3       2.493      Butyl  Phthalyl  Butyl Glycolate               36
  4       2.617      Diethyl  Hexyl  Phthalate                       2
  5      .2.747      C    ~  Terpineol                               1

-------
                                156
                             TABLE  B299
        Volatile  Organic  Compounds  Identified  in  Sample  No. 98S

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1      1.175        Cyclohexane                                   4
                             TABLE  B300
     Organic  Compounds  Identified in Acid  Extract of Sample No. 98A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.402
1.000
1.288
1.346


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
4
1
                             TABLE B301
    Organic Compounds  Identified  in Base Extract of Sample No.98B

       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       2.615      Diethyl  Hexyl  Phthalate                       1
  3       2.752      C15 -  Terpineol                               1

-------
                                157
                            TABLE B302

       Volatile Organic Compounds Identified in Sample No.99S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1     1.000       Chloroform                                   3

 2     1.174       Cyclohexane                                  4
                            TABLE B303

    Organic Compounds Identified in Acid Extract of Sample No. 99A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.379
0.663
1.000
1.104
1.346
1.367
1.416
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloroanisole
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
C,5 Terpineol
Approximate
Level
(ppb)
—
1
3
2
1
1
1

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                                158
                             TABLE B304
    Organic Compounds Identified  in Base Extract of Sample No.99B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       2.530      Diethyl  Hexyl  Phthalate                       1
  3       2.657      C15  - Terpineol                               1
                             TABLE B305
        Volatile Organic Compounds Identified in Sample  No. 100S
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.433
0.491
0.857
1.000
1.079 .
1.169
1.424
1.466
2.155
2.187
Compound
Ethanethiol
Acetone
Di-isopropyl Ether
Chloroform
Butanal
Cyclohexane
Dimethyl Bisulfide
Benzene + Trichloroethylene
C,Q Terpene
C,Q Terpene
Approximate
Level
(ppb)
19
1
1
46
6
2
19
1
1
85

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                           159
                        TABLE B306
Organic Compounds Identified in Acid Extract of Sample No.lOOA
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Relative
Retention
Time
0.610
0.662
0.670
0.752
0.770
0.802
0.811
0.871
0.886
0.907
0.931
0.943
0.976
1.985
1.000
1.033
1.051
1.099
1.138
1.150
1.156
1.171
1.186
1.201
1.210
1.224
1.236
1.275
1.305
1.311
1.326
Compound
Hydrocarbon C > 14
C15H24
Hydrocarbon C > 16
Hydrocarbon C > 16
Fatty Acid Methyl Ester C 12
Hydrocarbon C > 18
Hydrocarbon C > 18
Hydrocarbon C > 18
Fatty Acid Methyl Ester C 14
Tetrachl oroani sol e
Hydrocarbon C > 20
Fatty Acid Methyl Ester C > 15 +
Pentachloroanisole
Fatty Acid Methyl Ester C >_ 15
Hydrocarbon C ^ 20
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
Fatty Acid Methyl Ester C >_ 17
Methyl Stearate
Hydrocarbon C > 22
Fatty Acid Methyl Ester C 19
Terpene C 15
Cp-iH-pOp Methyl Pimarate Isomer
Cp-iH^oOp Methyl Pimarate Isomer
Fatty Acid Methyl Ester C 20
Cp^H-pOp Methyl Pimarate Isomer
Cp,H3pOp Methyl Pimarate Isomer
Cp-iH^pOp Methyl Pimarate Isomer
?
?
?
Fatty Acid Methyl Ester C > 23
Approximate
Level
(ppb)
1
8
1
1
1
1
5
6
7
1
1
4
2
1
34
12
7
62
13
5
5
16
27
58
18
22
36
340
5
5
8

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                           160
                     TABLE B306, cont.
Organic Compounds Identified in Acid Extract of Sample  No.lOOA  (continued)
Peak
No.
32
33
34
35
36
37
38
39
40
41
Relative
Retention
Time
1.344
1.365
1.383
1.398
1.404
1.413
1.425
1.443
1.478
1.569
Compound
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 24
?
?
?
Terpineol C 15
?
Fatty Acid Methyl Ester C > 26
?
CpiH32^2 Methyl Pimarate Isomer
Approximate
Level
(ppb)
18
36
16
18
18
8
10
12
5
3

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                           161
                        TABLE B307
Organic Compounds Identified in Base Extract  of Sample  No.lOOB
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Relative
Retention
Time
0.384
0.520
0.627
0.881
0.994
1.000
1.041
1.101
1.136
1.189
1.255
1.279
1.326
1.397
1.456
1.498
1.563
1.581
1.622
1.699
1.770
1.812
1.924
1.948
1.996
2.031
2.061
2.078
2.132
2.144
2.209
Compound
Diterpene C,QH,g
Diterpene C,QH,g
Diterpene C, -H, fi
Terpineol C 10
Hydroxylborneol
Camphor
Diterpene C,QH16
Dimethyl Styrene
Hydrocarbon C > 14
Hydrocarbon C > 14
Hydrocarbon C >_ 14
Triterpene C1t.H?.
Hydrocarbon C >_ 14
Triterpene C, 5H2«
Hydrocarbon C >_ 16
Hydrocarbon C > 16
Hydrocarbon C >_ 16
Hydrocarbon C >_ 16
Triterpene C, ,-H24
Hydrocarbon C ^ 18
?
Hydrocarbon C > 18
Hydrocarbon C >_ 20
Terpene C 15
Hydrocarbon C >_ 20
Hydrocarbon C >_ 20
?
?
Hydrocarbon C >_ 22
Dibutyl Phthalate
?
Approximate
Level
(ppb)
9
6
3
13
31
—
59
29
1
27
1
12
14
24
17
24
50
2
2
23
3
15
18
5
9
12
3
3
12
10
10

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                           162
                     TABLE B307, cont.
Organic Compounds Identified  in Base  Extract  of  Sample  No.lOOB  (continued)
Peak
No.
32
33
34
35
36
37
38
39
40
41
42
43
44
Relative
Retention
Time
2.245
2.256
2.292
2.345
2.376
2.384
2.404
2.422
2.434
2.446
2.570
2.630
2.750
Compound
Hydrocarbon C > 22
?
?
Hydrocarbon C > 24
Hydrocarbon C > 24
?
Hydrocarbon C > 24
?
?
?
Hydrocarbon C > 26
Diethyl Hexyl Phthalate
Terpineol C 15
Approximate
Level
(ppb)
3
7
2
10
7
51
3
40
4
5
3
3
3

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                               163
                            TABLE B308

       Volatile Organic Compounds Identified in Sample No. 101S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1     1.000       Chloroform                                   1

 2     1.176       Cyclohexane                                  1
                            TABLE B309

    Organic Compounds Identified in Acid Extract of Sample No.lOlA
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.412
1.000
1.103
1.212
1.288
1.352
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
5
3
1
3
1

-------
                                 164
                             TABLE B310
     Organic Compounds Identified in Base Extract of Sample No.lOlB

        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1      1.000      Camphor (IS)
  2      2.541      Diethyl Hexyl Phthalate                      1
  3      2.666      C c - Terpineol                              1
	12	——.	—_
                              TABLE  B311
        Volatile Organic Compounds Identified in Sample No. 102S

        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1       1.000      Chloroform                                   1
  2       1.265      Dioxolane                                    1
  3       1.821      Bromobenzene                                20

-------
                                165
                            TABLE B312
    Organic Compounds Identified in  Acid Extract of Sample No.lOZA
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.415
1.000
1.064
1.106
1.237
1.349
1.415
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
C,r Terpineol
Approximate
Level
(ppb)
—
3
1
2
2
2
1
                             TABLE  B313
    Organic Compounds  Identified in Base Extract of Sample No.1028

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1      1.000      Camphor (IS)
 2      2.535      Diethyl Hexyl Phthalate                      3

-------
                           166
                        TABLE B314
   Volatile  Organic Compounds  Identified in Sample No. 103S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.074
1.554
1.644
Compound
Chloroform
1,2-Dichloroethane
Dichlorobenzene
Dichloro benzene
Approximate
Level
(ppb)
1
1
1
21
                        TABLE B315
Organic Compounds Identified in  Acid Extract  of  Sample  N0.103A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.423 .
0.888
1.000
1.106
Compound
/
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myrsitate
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
—
1
2
1

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                                167
                            TABLE B316

    Organic Compounds Identified in Base Extract of Sample No.  103B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


                   No peaks over 1  PPB.
                             TABLE  B317

       Volatile Organic Compounds Identified in Sample N0.104S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
1.000
1.073
1.477
1.964
2.100
Compound
Chloroform
1 ,2-Dichloroethane
Trichloroethylene
Tetrachl oroethyl ene
Acetophenone
Approximate
Level
(ppb)
1
1
1
2
1

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                               168
                            TABLE B318

    Organic Compounds  Identified  in  Acid  Extract of Sample N0.104A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
Relative
Retention
Time
0.213
0.332
0.405
0.463
0.494
0.567
0.619
0.683
0.777
1.000
1.106
1.348
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
Dichlorobutane
Trichlorobutane
Trichloropentene
Trichlorohexane
Dichloroheptane
Trichlorohexane
Methyl Palmitate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
13
1
—
4
185
92
31
4
1
3
2
1
                            TABLE B319

    Organic Compounds Identified in Base Extract of Sample No. 104B
       Relative
Peak  Retention
No.      Time
Compound
Approximate
   Level
   (Ppb)
                   No peaks over 1 PPB.

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                         169
                     TABLE B320
Volatile Organic Compounds  Identified in Sample No.lOSS
Peak
No.
1
2
. 3
4
5
6

Relative
Retention
Time
1.000
1.076
1.238
1.433
1.514
2.022

Compound
Chloroform
1 ,2-Dichloroethane
Carbon Tetrachloride
Trichloropropane
Trichloroethylene
Tetrachl oroethyl ene
TABLE B321
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.391
0.887
0.945
1.000
1.064
1.104
1.141
1.205
1.229
1.242
1.278
1.352
1.376
1.422
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Pentachloroanisole
Methyl Palmitate
?
Methyl Stearate
?
Co-iH00Oo Methyl Pimarate Isomer
L\ 6L C.
C01H_000 Methyl Pimarate Isomer
L\ 3L L.
Methyl Dihydroabietate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C ^ 22
C1(- Terpineol
Approximate
Level
(ppb)
3
2
2
1
3
22

N0.105A
Approximate
Level
(ppb)
___
3
2
4
1
4
1
1
2
5
5
2
1
2

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                               170
                            TABLE B322

    Organic Compounds Identified in Base Extract of Sample No.  105B
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.843
1.000
1.106
1.285
1.319
1.676
2.040
2.498
Compound
?
Camphor (IS)
?
N,N-Di ethyl aniline
Chloroprene Dimer
Di ethyl Phthalate
Di butyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
—
3
3
3
2
1
1
                             TABLE B323
       Volatile Organic Compounds Identified in Sample N0.106S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1       1.000      Chloroform                                   5

 2       2.007      Tetrachloroethylene                          5
 3       2.078      C8H]4                                        1

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                            171
                        TABLE B324
Organic Compounds Identified in  Acid Extract  of Sample  No.106A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
Relative
Retention
Time
0.397
0.550
0.894
0.948
0.985
1.000
1.106
1.139
1.203
1.230
1.252
1.261
1.348
1.370
1.418
1.449
Compound
Methyl -2-Ethyl Hexanoate (IS)
CgH-jg Isomer
Methyl Myri state
Pentachloroanisole
?
Methyl Palmitate
Methyl Stearate
?
Fatty Acid Methyl Ester C >_ 20
7
Methyl Dehydroabietate
Butyl Phthalyl Butyl Glycolate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C >_ 22
C-|5 Terpineol
Fatty Acid Methyl Ester C >_ 24
Approximate
Level
(ppb)
— _ —
3
2
2
4
6
6
1
1
1
1
1
2
1
2
1

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                           172
                        TABLE B325
Organic Compounds Identified  in  Base  Extract of Sample No. 106B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
Relative
Retention
Time
0.531
0.830
1.000
1.107
1.322
1.508
1.571
1.662
1.690
1.769
1.865
2.051
2.086
2.408
2.465
2.521
2.544
2.617
2.645
2.685
2.758
2.837
2.922
2.970
Compound
CfiH-|g Isomer
?
Camphor (IS)
?
Chloroprene Isomer
Hydrocarbon C ^ 16
Dinitrotoluene
?
?
?
?
Di butyl Phthalate
Caffeine
Butyl Phthalyl Butyl Glycolate
Hydrocarbon C >_ 28
Diethyl Hexyl Phthalate
Hydrocarbon C >_ 29
Hydrocarbon C >_ 30
C,5 Terpineol
Hydrocarbon C >_ 31
Hydrocarbon C ^ 32
Hydrocarbon C >_ 33
Hydrocarbon C >_ 34
Hydrocarbon C >_ 35
Approximate
Level
(ppb)
3
1
—
1
1
2
22
17
20
5
2
1
1
1
1
2
1
1
2
1
1
1
1
1

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                           173
                        TABLE B326
   Volatile  Organic Compounds  Identified in Sample No. 107S

Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.492
1.991


Compound
Chloroform
Trichloroethylene
Tetrachl oroethyl ene
Approximate
Level
(ppb)
5
1
2
                        TABLE B327
Organic Compounds Identified  in  Acid  Extract  of  Sample No.l07A

Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.414
0.887
1.000
1.107
1.293
1.375


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myristate
Methyl Palmitate
Methyl Stearate
Fatty Acid Methyl Ester C >_ 22
?
Approximate
Level
(ppb)
—
1
3
4
1
1

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                                174
                            TABLE  B328

    Organic Compounds  Identified in Base Extract of Sample No.1078

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1      1.000      Camphor (IS)

 2      2.484      ?                                            1
 3      2.541      Diethyl Hexyl Phthalate                      3
 4      2.666      C,5 Terpineol                                1
                             TABLE B329

       Volatile Organic Compounds Identified in Sample No.lOSS


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform

  2       1.517      Trichloroethylene                            2

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                               175
                            TABLE B330
    Organic  Compounds  Identified  in  Acid  Extract  of  Sample  No. 108A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.439
0.900
1.000
1.121
1.230
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
C,r Terpene
Approximate
Level
(PPb)
—
2
5
3
2
                             TABLE  B331
    Organic Compounds  Identified in Base Extract of Sample No. 108B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

 1      1.000      Camphor (IS)
 2      1.740      Diethyl Phthalate                            4
 3      2.431       Butyl Phthalyl Butyl Glycolate               2

-------
                                176
                             TABLE B332
       Volatile Organic Compounds Identified in Sample No.1095

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   1
                             TABLE B333
    Organic Compounds Identified in Acid Extract of Sample N0.109A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.425
1.000
1.104
1.208


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,r Terpene
Approximate
Level
(ppb)
—
3
2
2
                             TABLE B334
     Organic Compounds  Identified  in  Base  Extract of Sample No. 109B

       Relative                                            Approximate
Peak   Retention                                              Level
 No.      Time       Compound                                  (ppb)

  1       1.000       Camphor  (IS)
  2       2.129       Dibutyl  Phthalate                            1
  3       2.618       Diethyl  Hexyl  Phthalate                      1

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                           177
                        TABLE B335
   Volatile  Organic Compounds  Identified in Sample No.llOS

Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.024
1.317
1.778


Compound
Chloroform
1 ,2-Dichloroethane
Bromo-Dichloromethane
Bromo benzene
Approximate
Level
(ppb)
4
1
2
13
                        TABLE B336
Organic Compounds Identified  in  Acid  Extract of Sample No.llOA
Peak
No.
1
2
3
4
Relative
Retention
Time
0.400
1.000
1.105
1.350
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ — —
2
1
1

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                               178
                            TABLE B337
    Organic Compounds Identified in Base Extract of Sample No.  HOB

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

                   No peaks over 1  PPB.
                             TABLE B338
       Volatile Organic Compounds Identified in Sample No.lllS
Peak
No.
1
2
3
4
Relative
Retention
Time
0.900
1.000
1.068
1.548
Compound
Dichloroethylene
Chloroform
1 ,2-Dichloroethane
?
Approximate
Level
(ppb)
4
10
2
1

-------
                               179
                            TABLE B339
   Organic Compounds Identified in Acid Extract of Sample No.lllA
Peak
No.
1
2
3
4
Relative
Retention
Time
0.411
1.000
1.102
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
5
2
2
                            TABLE B340
    Organic Compounds Identified in Base Extract of Sample No.  111B

D  L  DReJaVVe                                            Approximate
Peak  Retention                                               Level
 No.      Time       Compound
 1      1.000      Camphor (IS)
 2      2.569      Diethyl Hexyl  Phthalate                      2
 3      2.700      C,5 Terpineol                                 2
 4      2.837      ?                                            1
 5      3.001      ?                                            1

-------
                           180
                        TABLE B341
   Volatile  Organic Compounds  Identified in Sample No. 112S

Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.074
1.400
1.801
1.896
2.096


Compound
Chloroform
1 ,2-Dichloroethane
Trichloropropane
Dichlorobenzene
Dichlorobenzene
Dichlorobenzene
Approximate
Level
(ppb)
3
1
1
12
8
15
                        TABLE B342
Organic Compounds Identified in  Acid  Extract  of  Sample N0.112A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.376
1.000
1.105
1.346


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
4
1
1

-------
                                181
                            TABLE B343
    Organic Compounds Identified in Base Extract of Sample No. 112B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1      1.000      Camphor (IS)
 2      1.943      Atrazine                                     1
 3      2.617      Diethyl Hexyl Phthalate                      2
                             TABLE B344
       Volatile Organic Compounds Identified in Sample No.  113S

       Relative                                            Approximate
Peak   Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   1
  2       1.069      1,2-Dichloroethane                           2
  3       1.408      Trichloropropane                             1
  4       1.482      Trichloroethylene                            1
  5       1.930      Tetrachloroethylene                          7

-------
                                182
                             TABLE B345
    Organic Compounds Identified  in Acid Extract of Sample No.1 ISA


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1      0.415      Methyl-2-Ethyl Hexanoate  (IS)

  2      1.000      Methyl Palmitate                             3

  3      1.102      Methyl Stearate                              1
                             TABLE B346

     Organic Compounds Identified in Base Extract of Sample  No. 113B


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1       1.000       Camphor  (IS)

  2       2.573       Diethyl  Hexyl  Phthalate                      1

-------
                                183
                             TABLE B347

       Volatile Organic Compounds Identified in Sample N0.114S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1      1.000      Chloroform                                   4

  2      1.067      1,2-Dichloroethane                           1

  3      1.392      Trichloropropane                             1

  4      1.950      Tetrachloroethylene                          2
                             TABLE B348
     Organic  Compounds  Identified  in Acid  Extract of Sample No.IHA


       Relative                                            Approximate
Peak   Retention                                              Level
 No.      Time       Compound                                   (ppb)


  1       0.426      Methyl-2-Ethyl  Hexanoate  (IS)

  2       1.000      Methyl  Palmitate                             <1

  3       1.099      Methyl  Stearate                              1

-------
                               184
                            TABLE B349
    Organic Compounds Identified in Base Extract of Sample No. 114B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1      1.000      Camphor (IS)
 2      2.045      Dibutyl Phthalate                            2
                             TABLE B350
       Volatile Organic Compounds Identified in Sample No. 115S
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
1.000
1.068
1.304
1.403
1.477
1.555
1.964
Compound
Chloroform
1,2-Dichloroethane
Bromo-Dichloromethane
Trichloropropane
Trichloroethylene
Di bromo-Chl oromethane
Tetrachloroethylene
Approximate
Level
(ppb)
87
1
8
1
1
4
1

-------
                                185
                             TABLE B351
     Organic  Compounds  Identified  in Acid  Extract of Sample No.llSA

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1       0.410       Methyl-2-Ethyl  Hexanoate  (IS)
  2       1.000       Methyl  Palmitate                              2
                             TABLE B352
     Organic Compounds Identified in Base Extract of Sample No.  115B

        Relative                                            Approximate
 Peak  Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1       1.000       Camphor (IS)
  2       2.079       Dibutyl Phthalate                            1
                             TABLE B353
       Volatile Organic Compounds Identified) in Sample No.llGS

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound
  1       1.000       Chloroform                                   1
  2       1.068       1 ,2-Dichloroethane                           1

-------
                                186
                             TABLE B354

     Organic  Compounds  Identified  in Acid  Extract of Sample N0.116A

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1       0.425       Methyl-2-Ethyl  Hexanoate  (IS)
  2       1.000       Methyl  Palmitate                              3
  3       1.104       Methyl  Stearate                              1
                             TABLE B355

     Organic Compounds Identified in Base  Extract  of Sample  No.1166


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                         "           (ppb)


                    No peaks  over 1  PPB.
                             TABLE B356

       Volatile Organic Compounds Identified in Sample N0.117S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound


                   No  peaks  over  1 PPB.

-------
                                187
                             TABLE B357
    Organic Compounds Identified in Acid Extract of Sample No.lUA

       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)

  1       0.440      Methyl-2-Ethyl Hexanoate (IS)
  2       1.000      Methyl Palmitate                             2
                             TABLE B358
     Organic Compounds Identified in Base Extract  of Sample  No. H7B

        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1       1.000       Camphor  (IS)
  2       2.614       C15 Terpineol                                1
                             TABLE B359
        Volatile  Organic Compounds  Identified in Sample No. 118S

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time      Compound                                   (ppb)

  1       1.000     Chloroform                                   1
  2       1.627     Bromobenzene                                10

-------
                               188
                            TABLE B360
    Organic  Compounds  Identified  in Acid  Extract of Sample No.llSA
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.428
1.000
1.097
1.103
1.344
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Dibutyl Phthalate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
4
1
4
3
                             TABLE  B361

    Organic Compounds Identified in Base Extract of Sample No. 118B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


                   No peaks over 1  PPB.

-------
                                189
                             TABLE B362
       Volatile Organic Compounds Identified in Sample No. 119S

       Relative                                            Approximate
Peak   Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   3
  2       1.471      Trichloroethylene                            1
                             TABLE B363
     Organic  Compounds  Identified  in Acid  Extract of Sample No.H9A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.327
0.463
0.553
0.611
0.679
1.000
Compound
Methyl -2-Ethyl Hexanoate (IS)
Trichloropentane
Trichloropentane
Trichlorohexane
Trichloroheptane
Methyl Palmitate
Approximate
Level
(ppb)
—
23
12
15
9
2

-------
                                190
                            TABLE B364
    Organic Compounds Identified in Base Extract of Sample No. 119B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


 1      1.000      Camphor (IS)

 2      2.149      Dibutyl Phthalate                            1
                             TABLE B365
       Volatile Organic Compounds Identified in Sample No. 120S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   2

-------
                                191
                             TABLE B366
    Organic Compounds  Identified  in Acid Extract of Sample N0.120A


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time      Compound                                   (ppb)


  1      0.410      Methyl-2-Ethyl Hexanoate  (IS)
  2      1.000      Methyl  Palmitate                             2
                             TABLE B367
     Organic Compounds Identified in Base  Extract  of Sample  No. 120B

       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks over 1  PPB.
                             TABLE B368

       Volatile Organic Compounds Identified in Sample No. 121S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   n

-------
                            192
                        TABLE B369
Organic Compounds Identified  in  Acid  Extract of Sample N0.121A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
Relative
Retention
Time
0.162
0.281
0.370
0.406
0.449
0.526
0.596
0.666
0.731
0.795
0.859
0.917
0.972
1.000
1.028
1.083
1.132
1.181
1.226
1.272
1.315
Compound
Cg Alcohol
C7 Alcohol
Cg Alcohol
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
CIQ Alcohol
C^ Alcohol
C12 Alcohol
C,3 Alcohol
C,, Alcohol
C,r Alcohol
C]6 Alcohol
C17 Alcohol
Methyl Palmitate
C,g Alcohol
C-,g Alcohol
C2Q Alcohol
C,,., Alcohol
C22 Alcohol
C23 Alcohol
C0/1 Alcohol
Approximate
Level
(ppb)
2
2
6
—
8
15
• 10
8
8
9
5
4
2
1
2
2
2
2
2
2
1

-------
                                193
                             TABLE  B370

     Organic Compounds Identified in Base Extract of Sample  No. 121B


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                   No peaks  over 1  PPB.
                             TABLE B371

       Volatile Organic Compounds Identified in Sample No.  122S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   i
                             TABLE B372

     Organic  Compounds  Identified  in Acid Extract of Sample N0.122A


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (PPb)


  1       0.414      Methyl-2-Ethyl Hexanoate (IS)

  2       1.000      Methyl  Palmitate                              2

-------
                                194
                             TABLE B373
     Organic  Compounds  Identified  in  Base  Extract of Sample No. 122B


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks  over  1 PPB.
                             TABLE B374

       Volatile Organic Compounds Identified in Sample No. 123S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   2
                             TABLE B375
     Organic  Compounds  Identified  in  Acid  Extract  of Sample N0.123A


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1      0.449      Methyl-2-Ethyl Hexanoate (IS)

  2      1.000      Methyl  Palmitate                             2

  3      1.102      Methyl  Stearate                              1

-------
                                195
                             TABLE B376

     Organic Compounds Identified in Base  Extract  of Sample  No. 123B


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks over 1  PPB.
                             TABLE B377
       Volatile Organic Compounds Identified in Sample No.  124S

       Relative                                            Approximate
Peak   Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   1

-------
                                196
                            TABLE B378
    Organic  Compounds  Identified  in Acid  Extract of Sample N0.124A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.401
0.897
1.000
1.018
1.067
1.109
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
C,Q Terpineol
?
Methyl Stearate
Approximate
Level
(ppb)
___
1
3
2
2
4
                            TABLE B379

    Organic Compounds Identified in Base Extract of Sample No. 124B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Camphor (IS)

  2       2.565      Diethyl Hexyl Phthalate                      3

-------
                                197
                             TABLE B380
       Volatile Organic Compounds Identified in Sample No. 125S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1      1.000      Chloroform                                   n
                             TABLE B381
     Organic  Compounds  Identified  in Acid Extract of Sample N0.125A

Peak
No.
1
2
3
Relative
Retention
Time
0.423
1.000
1.100


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
—
2
2

-------
                                198
                            TABLE B382

     Organic  Compounds  Identified in Base Extract of Sample No. 125B
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.914
2.088
2.452
Compound
Camphor (IS)
Atrazine
Dibutyl Phthalate
Butyl Phthalyl Butyl Glycolate
Approximate
Level
(ppb)
___
1
2
1
                             TABLE B383
       Volatile Organic Compounds Identified in Sample No. 126S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)
 1      1.000      Chloroform                                   1

 2      2.298      Bromobenzene                                 5

-------
                                199
                             TABLE B384

    Organic Compounds Identified  in Acid Extract of Sample No.l26A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


  1       0.433      Methyl-2-Ethyl  Hexanoate  (IS)

  2       1.000      Methyl  Palmitate                             1
                             TABLE B385

     Organic Compounds Identified in Base Extract of Sample No.  126B


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks over 1  PPB.
                             TABLE B386
        Volatile Organic Compounds  Identified  in  Sample  No.  127S


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1       1.000      Chloroform                                    1

-------
                                200
                             TABLE B387

    Organic Compounds  Identified  in Acid Extract of Sample N0.127A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


  1       0.400      Methyl-2-Ethyl Hexanoate  (IS)

  2       1.000      Methyl Palmitate                             4

  3       1.111      Methyl Stearate                              5
                             TABLE B388
     Organic Compounds Identified in Base Extract of Sample No. 127B


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


 1      1.000      Camphor  (IS)

 2      1.942      Atrazine                                     1

-------
                                201
                             TABLE B389
       Volatile Organic Compounds Identified in Sample No. 128S
Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.357
1.633
2.232
Compound
Chloroform
Bromo-Dichloroethane
Di bromo-Chl oromethane
Dichloro benzene
^s"
Approximate
Level
(ppb)
40
10
8
10
                             TABLE B390
    Organic Compounds Identified in Acid Extract of Sample N0.128A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


                   No peaks  over  1 PPB.
                             TABLE B391

     Organic Compounds Identified in Base Extract of Sample No.  128B


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks over 1  PPB.

-------
                                202
                             TABLE B392
       Volatile Organic Compounds Identified in Sample No.  129S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   3
                             TABLE B393
     Organic  Compounds  Identified  in Acid  Extract of Sample No.  129A

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (PPb)


                    No peaks  over 1  PPB.
                             TABLE.B394

     Organic Compounds Identified in Base Extract of Sample No. 129B


        Relative                                            Approximate
 Peak  Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1      1.000      Camphor (IS)

  2      2.058      Dibutyl Phthalate                            2

-------
                                203
                             TABLE B395
       Volatile Organic Compounds Identified in Sample No. 130S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                  18

  2       2.159      Acetophenone                                 2
                             TABLE B396

     Organic  Compounds  Identified  in Acid  Extract of Sample No.  130A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.431
1.000
1.104
1.208
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
C,5 Terpene
Approximate
Level
(ppb)
_ —
2
1
1

-------
                                204
                            TABLE  B397
    Organic Compounds Identified in Base Extract of Sample No. 130B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No peaks over 1 PPB.
                             TABLE B398
       Volatile Organic Compounds Identified in Sample No. 131S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   1
  2       1.448      Dimethyl  Disulfide                           1

-------
                                205
                             TABLE  B399
    Organic Compounds Identified in Acid Extract of Sample No.lSIA
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.410
1.000
1.092
1.101
1.275
Compound
Methyl -2- Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
_ _ _
4
1
4
7
                             TABLE  B400
    Organic Compounds Identified in Base Extract of Sample No. 131B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       1.906      Atrazine                                     1
  3       2.028      ?                                            1
  4       2.074      Dibutyl  Phthalate                            1
  5       2.682      Diethyl  Hexyl Phthalate                      1

-------
                                 206
                             TABLE B401
       Volatile Organic Compounds Identified in Sample No.  132S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                  15
  2       2.076      Toluene                                      3
                             TABLE B402
    Organic Compounds Identified  in Acid Extract of Sample N0.132A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.424
1 . 000 .
1.031
1.101
1.132
1.350
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
C18 Alcohol
Methyl Stearate
Cp0 Alcohol
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— — —
5
1
5
1
1

-------
                                207
                             TABLE  B403
     Organic  Compounds  Identified in Base Extract of Sample No.1326
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.994
2.129
2.185
2.682
2.817
Compound
Camphor (IS)
Atrazine
?
Dibutyl Phthalate
Diethyl Hexyl Phthalate
C,5 Terpineol
Approximate
Level
(ppb)
—
1
1
1
1
1
                             TABLE B404
       Volatile Organic Compounds Identified in Sample No. 133S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Chloroform                                   4
  2       1.273      Cyclohexane                                  1
  3       1.506      Dimethyl  Disulfide                           1

-------
                                208
                             TABLE B405
    Organic Compounds Identified  in Acid Extract of Sample N0.133A

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       0.431      Methyl-2-Ethyl  Hexanoate  (IS)
  2       1.000      Methyl  Pa Imitate                             2
  3       1.104      Methyl  Stearate                             3
                             TABLE B406
     Organic Compounds Identified in Base Extract of Sample No.  133B

        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

  1      1.000      Camphor (IS)
  2      2.104      Dibutyl Phthalate                            1
  3      2.575      Diethyl Hexyl Phthalate                      1
  4      2.708      C15 Terpineol                                1

-------
                                209
                             TABLE B407

       Volatile Organic Compounds Identified in Sample No. 134S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks over  1 PPB.
                             TABLE B408
     Organic  Compounds  Identified  in Acid Extract of Sample N0.134A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.430
0.908
1.000
1.089
1.110
1.126
1.218
1.288
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
C,,- Terpene
C,5 Terpene
Butyl Phthalyl Butyl Glycolate
Approximate
Level
(ppb)
—
2
5
4
4
3
2
3

-------
                                210
                             TABLE  B409
    Organic Compounds  Identified in Base Extract of Sample No. 134B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       1.000      Camphor  (IS)
  2       2.117      Dibutyl  Phthalate                            1
  3       2.590      Diethyl  Hexyl Phthalate                      1
  4       2.725      C]5 Terpineol                                1
                             TABLE B410
        Volatile Organic Compounds Identified in Sample No. 135S

       Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

   1      1.000      Chloroform                                   1
   2      1.071       1,2-Dichloroethane                           2
   3      1.547      Benzene                                      3

-------
                                211
                             TABLE  B411
     Organic  Compounds  Identified in Acid  Extract of Sample No. 135A

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

   1      0.391       Methyl-2-Ethyl  Hexanoate  (IS)
   2      1.000       Methyl  Palmitate                              2
   3      1.107       Methyl  Stearate                              1
   4      1.359       Diethyl Hexyl Phthalate                       1
                             TABLE  B412
    Organic Compounds Identified in Base Extract of Sample No. 135B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

   1      1.000      Camphor  (IS)
   2      1.576      C,Q Terpineol                                 1
   3      2.606      Diethyl  Hexyl Phthalate                       1

-------
                               212
                            TABLE B413
       Volatile Organic Compounds Identified in Sample No. 136S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1     1.000      Chloroform                                   1
  2     1.071      1,2-Dichloroethane                           3
  3     1.296      Dichlorobenzene                              1
                             TABLE  B414
     Organic Compounds  Identified in Acid  Extract of Sample No. 136A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.373
0.814
1.000
1.100
1.343
Compound
Methyl -2-Ethyl Hexanoate (IS)
C.Q Terpineol
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
___
1
6
3
4

-------
                                213
                            TABLE  B415
    Organic Compounds Identified in Base Extract of Sample No.1366

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1     1.000      Camphor (IS)
  2     1.516      C]0 Terpineol                                1
                             TABLE B416

        Volatile Organic Compounds Identified in Sample No. 137S

Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.490
1.630


Compound
Chloroform
Benzene
Hexane
Approximate
Level
(ppb)
1
2
2

-------
                               214
                            TABLE B417
    Organic Compounds Identified in Acid Extract of Sample No. 137A
Peak
No.
1
2
3
4
5
6
7
8
Relative
Retention
Time
0.379
0.818
0.912
1.000
1.100
1.118
1.205
1.341
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
C,Q Terpineol
Methyl Palmitate
Methyl Stearate
C,5 Terpene
C,,- Terpene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)

2
2
5
2
1
1
1
                             TABLE  B418
    Organic Compounds Identified in Base Extract of Sample No. 137B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (PPb)

  1     1.000      Camphor (IS)
  2     2.500      Diethyl Hexyl Phthalate                      1

-------
                               215
                            TABLE B419
       Volatile Organic Compounds Identified in Sample No. 138S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1     1.000      Chloroform                                   1
  2     1.501      Benzene                                      1
  3     1.636      Hexane                                       1
                             TABLE  B420
     Organic  Compounds  Identified in Acid Extract of Sample No. 138A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.380
0.823
0.891
0.947
1.000
1.094
1.332
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpinebl
Methyl Myri state
Fatty Acid Methyl Ester C >_ 14
Methyl Pa Imitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— _
1
3
1
13
6
2

-------
                                216
                             TABLE  B421
    Organic Compounds Identified in Base Extract of Sample No. 138B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


  1     1.000      Camphor (IS)

  2     2.495      Diethyl Hexyl Phthalate                      4
                             TABLE B422

        Volatile Organic Compounds Identified  in  Sample  No. 139S
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.467
0.817
1.000
1.302
1.479
1.555
Compound
Acetone
Pentene
Chloroform
Bromo-Di chl oromethane
Trichloroethylene
Di bromo-Chl oromethane
Approximate
Level
(ppb)
1
1
40
7
5
7

-------
                               217
                            TABLE B423

    Organic Compounds Identified in Acid Extract of Sample No. I39A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.380
1.000
1.102
1.341
1.407
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
C,,- Terpineol
Approximate
Level
(ppb)
— — _
2
1
1
4
                             TABLE  B424

    Organic Compounds Identified in Base Extract of Sample No. 139B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No peaks over 1 PPB.

-------
                           218
                       TABLE B425
   Volatile  Organic  Compounds Identified  in Sample No. 140S

Peak
No.
1
2
3
4
Relative
Retention
Time
1.000
1.302
1.490
2.077


Compound
Chloroform
Chloroprene
Trichloroethylene
Toluene
Approximate
Level
(ppb)
1
1
1
2
                        TABLE B426
Organic Compounds Identified in Acid Extract of Sample  No. 140A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.193
0.401
1.000
1.101
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
—
3
5

-------
                                219
                             TABLE  B427
    Organic Compounds Identified in Base Extract of Sample No.1408

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No peaks  over 1 PPB.
                             TABLE B428

        Volatile Organic Compounds Identified in Sample No. 141S
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.386
1.000
1.219
1.493
2.084
Compound
Dichloromethane
Chloroform
Carbon Tetrachloride
Trichloroethylene
Toluene
Approximate
Level
(ppb)
1
1
1
1
1

-------
                                220
                             TABLE  B429
    Organic Compounds  Identified in Acid Extract of Sample No. 141A

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1     0.390      Methyl-2-Ethyl  Hexanoate (IS)
  2     1.000      Methyl Palmitate                             3
  3     1.099      Methyl Stearate                              3
  4     1.338      Diethyl Hexyl Phthalate                      1
                             TABLE B430
     Organic Compounds Identified in  Base  Extract  of Sample  No.  141B

       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

   1      1.000       Camphor (IS)
   2      2.570       Diethyl  Hexyl  Phthalate                       1

-------
                        221
                     TABLE B431
Volatile Organic Compounds Identified in Sample No. 142S
Peak
No.
1
2
3
4
5
6
7
8
9
10
11

Relative
Retention
Time
0.357
0.423
1.000
1.061
.1.091
1.187
1.258
1.400
1.409
1.476
1.931

Compound
Dichloromethane
Acetone
Chloroform
1 ,2-Dichloroethane
Methacrylonitrile
Carbon Tetrachloride
Bromo-Di chl oromethane
Trichloroethylene
Benzene
Bromo-Trichloropropane
Toluene
TABLE B432
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
3
4
Relative
Retention
Time
0.390
1.000
1.098
1.337
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
3
3
1
1
2
1
1
1
2
1

of Sample No. 142A
Approximate
Level
(ppb)
— — •
2
1
3

-------
                                222
                             TABLE B433

    Organic Compounds Identified  in Base Extract of Sample No. 142B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


   1      1.000      Camphor  (IS)

   2      2.115      Diethyl  Hexyl  Phthalate                      2
                             TABLE B434
         Volatile  Organic  Compounds Identified in Sample No. 143S


        Relative                                            Approximate
 Peak   Retention                                                Level
 No.      Time      Compound                                    (ppb)


                    No peaks over 1. PPB.

-------
                                223
                            TABLE B435
    Organic Compounds Identified in Acid Extract of Sample No. 143A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


   1      0.419      Methyl-2-Ethyl Hexanoate  (IS)

   2      1.000      Methyl Palmitate                             2

   3      1.102      Methyl Stearate                              1
                             TABLE  B436
    Organic Compounds Identified in Base Extract of Sample No. 143B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1     1.000      Camphor (IS)

  2     2.057      Dibutyl Phthalate                            1
                            I TABLE B437

        Volatile Organic Compounds Identified  in  Sample  No. 144S


       Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


   1      1.000      Chloroform                                   2

-------
                                224
                             TABLE  B438
    Organic Compounds  Identified in Acid Extract of Sample No. 144A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


   1      0.400      Methyl-2-Ethyl  Hexanoate  (IS)

   2      1.339      Diethyl Hexyl Phthalate                       1
                             TABLE B439
     Organic  Compounds  Identified  in  Base  Extract of Sample No.l44B


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No  peaks  over  1  PPB.
                             TABLE B440
        Volatile Organic Compounds Identified in Sample No. 145S
Peak
No.
1
2
3
4
Relative
Retention
Time
1 . 000
1.236
1.330
1.599
Compound
Chloroform
Carbon Tetrachloride
Bromo-Dichloromethane
Dibromo-Chloromethane
Approximate
Level
(ppb)
43
3
7
5

-------
                               225
                            TABLE B441

    Organic Compounds Identified in Acid Extract of Sample No.  145A
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
0.326
0.492
1.000
1.091
1.238
1.335
1.354
1.372
1.381
1.406
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Dioctyl Adi pate
Diethyl Hexyl Phthalate Isomers
Diethyl Hexyl Phthalate Isomers
Diethyl Hexyl Phthalate Isomers
Diethyl Hexyl Phthalate Isomers
C15 Terpineol
Approximate
Level
(ppb)
1
—
4
4
86
4
6
17
26
1
                             TABLE  B442
    Organic Compounds Identified in Base Extract of Sample No. 145B
       Relative
Peak  Retention
No.      Time
Compound
Approximate
   Level
   (ppb)
                   No peaks over 1 PPB.

-------
                               226
                            TABLE B443
       Volatile Organic Compounds Identified in Sample No. 146S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1     1.000      Chloroform                                   1

  2     1.279      Bromo-Dichloromethane                        1
                             TABLE  B444
     Organic  Compounds  Identified in Acid Extract of Sample No. 146A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.271
0.412
1.000
1.088
1.099
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Approximate
Level
(ppb)
1
—
5
1
2

-------
                                227
                             TABLE  B445

    Organic Compounds Identified in Base Extract of Sample No. 146B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1                No peaks  over 1 PPB.
                             TABLE B446
        Volatile Organic Compounds Identified in Sample No.147S
Peak
No.
1
2
3
4
Relative
Retention
Time
0.422
1.000
1.319
1.583
Compound
Acetone
Chloroform
Bromo-Di chl oromethane
Dibromo-chloromethane
Approximate
Level
(ppb)
1
38
14
4

-------
                               228
                            TABLE B447
    Organic Compounds Identified in Acid Extract of Sample No. 147A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.410
1.000
1.089
1.100
1.236
1.340
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Dioctyl Adi pate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
	
5
1
3
4
1
                             TABLE  B448
    Organic Compounds Identified in Base Extract of Sample No. 147B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

   1      1.000      Camphor  (IS)  .
   2      2.011      Dibutyl  Phthalate                            1
   3      2.461      Diethyl  Hexyl Phthalate                      1

-------
                                229
                            TABLE B449

       Volatile Organic Compounds Identified in Sample No. 148S


       Relative                                            Approximate
Peak   Retention                                                Level
No.      Time      Compound                                    (ppb)


  1     1.359       Bromo-Dichloromethane                         3
                             TABLE  B450

    Organic Compounds  Identified in Acid Extract of Sample No. 148A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


  1     0.341      1,1 ,2,2-Tetrachloroethane                    2

  2     0.430      Methyl-2-Ethyl Hexanoate (IS)
                          TABLE B451
    Organic Compounds  Identified in Base Extract of Sample No. I486


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


   1      1.000      Camphor  (IS)

   2      2.011      Dibutyl  Phthalate                             1

-------
                             230
                          TABLE B452

       Volatile Organic Compounds Identified in Sample No.149S


       Relative                                            Approximate
Peak  Retention                         .                      Level
No.      Time      Compound                                   (ppb)


  1      1.000      Chloroform                                   6

  2      1.500      Benzene                                      2
                          TABLE B453
    Organic Compounds Identified in Acid Extract of Sample No. 149A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.418
1.000
1.009
1.100


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
C,r Terpene
Methyl Stearate
Approximate
Level
(ppb)
—
2
1
2
                          TABLE B454

    Organic Compounds Identified in Base Extract of Sample No. 149B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


                   No peaks over 1 PPB.

-------
                             231
                          TABLE B455

       Volatile Organic Compounds Identified in Sample No. 150S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


   1     0.402      Dichloromethane                              2

   2     1.000      Chloroform                                   2
                          TABLE B456

    Organic Compounds  Identified in Acid Extract of Sample No. 150A
Peak
No.
1
2
3
Relative
Retention
Time
0.410
1.000
1.108
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
—
1
1
                          TABLE B457
     Organic  Compounds  Identified  in Base Extract of Sample No. 150B

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No  peaks  over  1 PPB.

-------
                              232
                          TABLE B458
        Volatile  Organic  Compounds  Identified  in Sample No. 151S

       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)

                    No peaks over 1 PPB.
                            TABLE B459
     Organic Compounds  Identified  in Acid  Extract of Sample No. 151A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.410
0.850
0.955
1.000
1.102
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
?
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
~ -. -»
102
64
11
4
                          TABLE B460
    Organic Compounds Identified in Base Extract of Sample No. 151B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

   1      1.000      Camphor  (IS)
   2      2.449      Diethyl  Hexyl Phthalate                      1

-------
                              233
                          TABLE B461

       Volatile Organic Compounds  Identified in Sample No. 152S


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time      Compound                                    (ppb)


                   No  peaks  over  1  PPB.
                          TABLE B462

     Organic  Compounds  Identified  in Acid Extract of Sample No. 152A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.419
1.000
1.098
1.329


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— — .
6
3
2
                          TABLE B463

    Organic Compounds Identified in Base Extract of Sample No. 152B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


   1      1.000      Camphor (IS)

   2      2.009      Dibutyl Phthalate                            1

-------
                         234
                     TABLE B464
   Volatile Organic Compounds Identified in Sample No. 153S
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.335
1.588
Compound
Chloroform
Bromo-Dichloromethane
Dibromo-Chloromethane
Approximate
Level
(ppb)
24
4
4
                      TABLE  B465
Organic Compounds Identified in Acid Extract  of  Sample  No. 153A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.362
0.435
0.471
0.543
0.610
0.676
0.740
0.800
0.861
0.921
0.976
Compound
Cg Alcohol
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
C,Q Alcohol
C^ Alcohol
C]2 Alcohol
C13 Alcohol
C14 Alcohol
C-|5 Alcohol
C,c Alcohol
1 D
C,-, Alcohol
Approximate
Level
(ppb)
2
—
7
8
9
7
6
8
5
4
1

-------
                              235
                          TABLE B466

    Organic Compounds  Identified in Base Extract of Sample No.1538


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks over 1 PPB.
                          TABLE B467

        Volatile  Organic  Compounds  Identified  in  Sample  No. 154S


       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)
                    No peaks  over 1  PPB.
                               TABLE B468
     Organic  Compounds  Identified  in Acid Extract  of  Sample  No. 154A


       Relative                                             Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)

                   No peaks over 1  PPB.

-------
                              236
                          TABLE B469
    Organic Compounds Identified in Base Extract of Sample No. 154B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1     1.000      Camphor (IS)

  2.    2.043      Diethyl Hexyl Phthalate                      2
                          TABLE B470

        Volatile Organic Compounds  Identified  in  Sample  No. 155S


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks over  1  PPB.
                          TABLE B471

     Organic Compounds Identified  in Acid  Extract  of  Sample  No. 155A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.412
1.000
1.105
1.187
1.146
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Unidentified Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
2
2
3
. 4

-------
                              237
                          TABLE B472
    Organic Compounds  Identified in Base Extract of Sample No.l55B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks over 1 PPB.
                          TABLE B473

        Volatile Organic Compounds  Identified  in  Sample  No. 156S

Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.330
1.588
<

Compound
Chloroform
Bromo-Dichloromethane
Di bromo-Chl oromethane
Approximate
Level
(ppb)
29
2
2
                          TABLE B474

     Organic  Compounds  Identified  in Acid  Extract of Sample N0.156A


       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)


   1      0.420       Methyl-2-Ethyl  Hexanoate  (IS)

   2      1.000       Methyl  Palmitate                              3

   3      1.107       Methyl  Stearate                              2

-------
                              238
                          TABLE B475
    Organic Compounds Identified in Base Extract of Sample No. 156B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

   1      1.000      Camphor  (IS)
   2      2.023      Dibutyl  Phthalate                            2
   3      2.470      Diethyl  Hexyl Phthalate                      1
                           TABLE  B476
        Volatile Organic Compounds Identified in Sample No. 157S

        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)

   1     1.500      Trichloroethylene                            1

-------
                         239
                      TABLE  B477
Organic Compounds Identified in Acid Extract  of Sample  No. 157A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.434
0.910
1.000
1.102
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,r Terpene
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
— _ _
1
3
3
                      TABLE B478
Organic Compounds Identified in Base  Extract  of  Sample  No.l57B
Peak
No.
1
2
3
4
5
6
7
8
9
10
Relative
Retention
Time
1.000
2.023
2.415
2.470
2.559
2.597
2.631
2.696
2.774
2.857
Compound
Camphor (IS)


Dibutyl Phthalate
Hydrocarbon C
Di ethyl Hexyl
Hydrocarbon C
C,g Terpineol
Hydrocarbon C
Hydrocarbon C
Hydrocarbon C
Hydrocarbon C
1 24
Phthalate
I26
1 28
> 28
>_ 30
>_ 30
Approximate
Level
(ppb)
—
5
1
2
1
2
1
1
1
1

-------
                              240
                          TABLE B479
        Volatile Organic Compounds Identified in Sample No. 158S


       Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


   1      1-000      Chloroform                                   c
                          TABLE B480

    Organic Compounds Identified in Acid Extract of Sample No. 158A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.420
0.896
1.000
1.107
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Myri state
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
___
6
16
2
                          TABLE B481
    Organic Compounds Identified in Base Extract of Sample N0.158B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound
                   No peaks over 1 PPB.

-------
                              241
                          TABLE B482

        Volatile  Organic Compounds  Identified in Sample No. 159S


       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)


                    No  peaks over 1  PPB.
                          TABLE B483
    Organic Compounds  Identified in Acid Extract of Sample No. 159A

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1     0.420      Methyl-2-Ethyl Hexanoate (IS)
  2     1.000      Methyl Palmitate                             6
  3     1.103      Methyl Stearate                              4
                          TABLE B484

    Organic Compounds  Identified in Base Extract of Sample No. 159B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No peaks over 1  PPB.

-------
                              242
                         TABLE  B485

        Volatile  Organic Compounds  Identified in Sample No. 160S


       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)


   1      1.000       Chloroform                                   7
                          TABLE B486
    Organic Compounds  Identified in Acid Extract of Sample No. 160A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


                   No  peaks over 1  PPB.
                          TABLE B487
     Organic Compounds  Identified  in  Base  Extract of  Sample No. 160B


       Relative                                  .         Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                    (ppb)


                    No  peaks  over  1 PPB.

-------
                             243
                          TABLE B488

        Volatile Organic Compounds Identified  in  Sample  No. 161S


       Relative                                            Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks over 1  PPB.
                          TABLE B489

     Organic  Compounds  Identified  in Acid Extract of Sample No. 161A


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No  peaks over  1 PPB.
                          TABLE B490
    Organic Compounds Identified in Base Extract of Sample No. 161B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No peaks over 1  PPB.

-------
                              244
                          TABLE B491
        Volatile  Organic  Compounds  Identified  in  Sample  No. 162S


       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)

  1      1.000        Chloroform                                   2
                          TABLE B492
     Organic Compounds Identified  in Acid  Extract  of  Sample  No. 162A


       Relative                                             Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)


                      No peaks over 1 PPB.
                          TABLE B493
    Organic Compounds Identified in Base Extract of Sample No.l62B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (PPb)


                       No peaks over 1 PPB.

-------
                              245
                          TABLE B494
        Volatile  Organic  Compounds  Identified  in Sample No. 163S


       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)
                     No peaks over 1 PPB.
                          TABLE B495

     Organic  Compounds  Identified in Acid Extract of Sample No. 163A
Peak
No.
1
2
3
Relative
Retention
Time
0.321
0.420
1.000
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Approximate
Level
(ppb)
1
—
2
                          TABLE B496
    Organic Compounds Identified in Base Extract of Sample No.1638

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1     1.000       Camphor  (IS)

  2     2.496       Diethyl  Hexyl Phthalate                     1

-------
                              246
                          TABLE B497

        Volatile Organic Compounds Identified  in Sample No. 164S


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)
                        No peaks over 1  PPB.
                          TABLE B498

     Organic  Compounds  Identified  in Acid Extract of Sample No.l64A


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                      No peaks over 1  PPB.
                          TABLE B499
    Organic Compounds  Identified in Base Extract of Sample No. 164B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1     1.000       Camphor  (IS)

 2     1.983       Diisobutyl  Phthalate                         4
 3     2.092       Dibutyl  Phthalate                            7

-------
                              247
                          TABLE B500

        Volatile Organic  Compounds  Identified  in Sample  No. 165S


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                    (ppb)


  1      0.846       Tetrahydrofuran                              3

  2      1.000       Chloroform                                   4

  3      1.618       Hexanol                                       2
                          TABLE B501

     Organic Compounds Identified  in Acid  Extract  of  Sample  No. 165A


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                    (ppb)


                      No peaks over 1 PPB.
                          TABLE B502
    Organic Compounds Identified in Base Extract of Sample No. 165B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                      No peaks over 1 PPB.

-------
                              248
                          TABLE  B503
       Volatile Organic Compounds  Identified in Sample No. 166S


       Relative                                            Approximate
Peak   Retention                                               Level
No.      Time      Compound                                   (ppb)
                       No peaks over 1  PPB.
                          TABLE B504
    Organic Compounds  Identified in Acid Extract of Sample No. 166A


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                       No peaks over 1  PPB.
                          TABLE B505
    Organic Compounds Identified in Base Extract of Sample No. 166B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                      No  peaks over 1 PPB.

-------
                              249
                          TABLE B506

        Volatile  Organic Compounds  Identified in Sample No. 167S
Peak
No.
1
2
Relative
Retention
Time
0.390
1.465
Compound
Dichloromethane
Benzene
Approximate
Level
(ppb)
5
1
                          TABLE B507

     Organic  Compounds  Identified in Acid Extract of Sample No. 167A

Peak
No.
1
2
3
Relative
Retention
Time
0.387
1.000
1.288


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Butyl Phthalyl Butyl Glycolate
Approximate
Level
(ppb)
—
2
2
                          TABLE B508
    Organic Compounds Identified in Base Extract of Sample No. 167B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                      No peaks over 1 PPB.

-------
                      250
                  TABUE B509
Volatile Organic Compounds Identified  in  Sample  No. 168S
Peak
No.
1
2
3
4
5
6
7

Relative
Retention
Time
0.879
0.949
1.000
1.440
1 . 546
1.919
2.026

Compound
Tetrahydrofuran
1 ,2-Dichloroethane
Chloroform
Trichloroethylene
Methyl -t-Butyl Ketone
Tetrachl oroethyl ene
Dichlorobenzene
TABLE B510
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
Relative
Retention
Time
0.349
0.434
0.568
0.678
0.705
0.781
0.933
0.969
1.000
1.103
1.140
1.255
1.346
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Pentachlorobutene
CxHyClz, x ^4, z i 5
CxHyC1z' x ^4, z i 5
Pentachloroethane
Hexachlorobenzene
?
Methyl Palmitate
Methyl Stearate
?
?
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
318
4
9
188
1
45
2

of Sample N0.168A
Approximate
Level
(ppb)
1
—
1
6
7
1
3
2
3
2
1
3
1

-------
                         251
                     TABLE B511
Organic Compounds Identified  in Base Extract of Sample No. 168B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15

16

17

18

19

20
21
22
23
Relative
Retention
Time
0.580
0.762
0.784
0.817
0.878
0.917
0.934
0.955
0.972
1.000
1.016
1.083
1.127
1.182
1.221

1.271

1.359

1.387

1.409

1.448
1.503
1.691
2.420
Compound
Tetrachloroe thane
Hexachloroethane
Tetrachlorobutadiene
Tetrachl orobutadi ene
Pentachlorobutadiene
Tetrachlorobutadiene
Pentachlorobutadiene
Pentachlorobutadiene
He xachl orobutadi ene
Camphor (IS)
Pentachlorobutene
Pentachlorobutene
Hexachlorobutene
Hexachlorobutene
C H Cl , x > 4, z > 5
x y z — —
CH Cl . x > 4, z > 5
x y z — —
C H Cl . x > 4, z > 5
x y z — —
C H Cl , x > 4, z > 5
x y z — —
C H Cl , x > 4, z > 5
x y z - -
Pentachloroethane
Pentachloroe thane
Hexachlorobenzene
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
44
3
5
7
6
11
5
38
22
—
64
27
21
17
99

100

14

3

13

1
2
4
2

-------
                              252
                          TABLE  B512

       Volatile Organic Compounds Identified in Sample No. 169S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1     0.877       Tetrahydrofuran                              2
                          TABLE B513

    Organic Compounds Identified in Acid Extract of Sample No. 169A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.352
0.431
1.000
1.021
1.104
1.239
1.376
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
?
?
?
Approximate
Level
(ppb)
1
—
5
1
2
4
1

-------
                             253
                         TABLE B514
    Organic Compounds Identified  in Base Extract of Sample  No.l69B
Peak
No.
1
2
3
Relative
Retention
Time
1.000
1.147
1.413
Compound
Camphor (IS)
2-Methyl Thiobenzothiazole
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
3
1
                          TABLE  B515
       Volatile Organic Compounds Identified in Sample No.170S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)
                      No peaks over 1 PPB.
                          TABLE  B516

    Organic Compounds Identified in Acid Extract of Sample No. 170A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.410
1.000
1.065
1.108
1.244
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Approximate
Level
(ppb)
—
3
1
3
3

-------
                              254
                          TABLE B517
    Organic Compounds Identified in Base Extract of Sample No. 170B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1      1.000       Camphor  (IS)

  2      2.081       Dibutyl  Phthalate                             1

  3      2.561       Diethyl  Hexyl Phthalate                       1
                          TABLE B518

        Volatile Organic Compounds Identified in Sample No. 171S


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                       No peaks over 1 PPB.

-------
                         255
                     TABLE B519
Organic Compounds Identified  in Acid Extract of Sample  No. 171A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24

25
26
Relative
Retention
Time
0.306
0.324
0.420
0.420
0.468
0.543
0.612
0.678
0.742
0.805
0.865
0.892
0.922
0.979
1.000
1.033
1.084
1.102
1.129
1.180
1.222
1.267
1.309
1.348

1.387
1.414
Compound
C7 Alcohol
Dichlorobutene
Cg Alcohol
Methyl -2- Ethyl Hexanoate (IS)
Cg Alcohol
C-JQ Alcohol
C^ Alcohol
C]2 Alcohol
C13 Alcohol
C,. Alcohol
C15 Alcohol
Methyl Myri state
C]6 Alcohol
C17 Alcohol
Methyl Palmitate
C18 Alcohol
C,g Alcohol
Methyl Stearate
C2Q Alcohol
C21 Alcohol
C22 Alcohol
C23 Alcohol
C24 Alcohol
Diethyl Hexyl Phthalate +
C25 Alcohol
C26 Alcohol
C Terpineol
Approximate
Level
(ppb)
1
1
1
—
2
2
2
3
3
3
3
1
3
4
12
6
4
16
7
5
6
4
3

3
2
1

-------
                             256
                         TABLE  B520
    Organic Compounds  Identified in Base  Extract  of  Sample  No.l71B
Peak
No.
1
2
3
Relative
Retention
Time
1.000
2.019
2.500
Compound
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— _ _
1
1
                          TABLE B521

       Volatile Organic Compounds Identified in Sample No. 172S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                       No  peaks over  1  PPB.
                          TABLE B522

     Organic  Compounds  Identified  in Acid  Extract  of  Sample No. 172A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.342
0.421
1.000
1.107
1.355
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
—
6
8
6

-------
                              257
                          TABLE B523
    Organic Compounds Identified in Base Extract of Sample No. 172B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                      No peaks over 1  PPB.
                          TABLE B524

        Volatile Organic Compounds  Identified  in  Sample  No. 173S

Peak
No.
1
Relative
Retention
Time
1.000


Compound
Chloroform
Approximate
Level
(ppb)
4
                          TABLE B525

     Organic Compounds  Identified  in Acid  Extract  of  Sample  No. 173A


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                    (ppb)


  1      0.411        Methyl-2-Ethyl  Hexanoate (IS)

  2      1.000       Methyl  Palmitate                              2

  3      1.107       Methyl  Stearate                              1

-------
                              258
                          TABLE B526
    Organic Compounds  Identified in Base Extract of Sample No.1736


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1      1.000       Camphor  (IS)

  2      2.001       Dibutyl  Phthalate                            2
                           TABLE  B527
        Volatile Organic Compounds Identified  in  Sample  No. 174S


       Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1      1.000       Chloroform                                   1
                           TABLE  B528

     Organic Compounds Identified in Acid  Extract  of  Sample  No. 174A


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                      No peaks over 1  PPB.

-------
                              259
                          TABLE B529
    Organic Compounds Identified in Base Extract of Sample No. 174B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound            "                       (ppb)


                      No peaks over 1 PPB.
                           TABLE  B530
        Volatile Organic Compounds Identified in Sample No.l75S


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                       No  peaks over 1 PPB.
                           TABLE B531
     Organic Compounds Identified in Acid Extract of Sample  No. USA


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.     Time       Compound                                   (ppb)


  1     0.427       Methyl-2-Ethyl Hexanoate (IS)

  2     1.000       Methyl PaImitate                             1
  3     1.104       Methyl Stearate                              1

-------
                              260
                          TABLE  B532
    Organic Compounds Identified in Base Extract of Sample No.1756


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                      No peaks over 1  PPB.
                           TABLE B533

        Volatile Organic Compounds Identified in Sample No.176S
Peak
No.
1
2
3
4
Relative
Retention
Time
0.397
0.673
1.000
1.459
Compound
Dimethyl Sulfide
Di me thoxyme thane
Chloroform
Dimethyl Disulfide
Approximate
Level
(ppb)
1
3
1
1
                           TABLE B534

     Organic Compounds Identified in Acid Extract of Sample  No.l76A


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1      1.000      Methyl Palmitate                             6

  2      1.104      Methyl Stearate                              3

  3      1.120      C   ~ TerPene                                1

-------
                              261
                           TABLE  B535

    Organic Compounds  Identified in Base Extract of Sample No.1768


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

 1     1.000       Camphor  (IS)

 2     2.082       Dibutyl  Phthalate                             1

 3     2.563       Diethyl  Hexyl Phthalate                       1
                           TABLE  B536
        Volatile Organic  Compounds  Identified  in  Sample  No. 177S

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                    (ppb)


                       No peaks over 1 PPB.

-------
                               262
                           TABLE B537

     Organic  Compounds  Identified  in  Acid  Extract  of Sample No. 177A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
Relative
Retention
Time
0.426
0.475
0.543
0.607
0.678
0.739
0.801
0.862
0.920
0.975
1.031
Compound
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
C,Q Alcohol
C,, Alcohol
C,2 Alcohol
C,3 Alcohol
C,. Alcohol
C-|5 Alcohol
C16 Alcohol
C,7 Alcohol
C-jg Alcohol
Approximate
Level
(ppb)
—
1
1
1
4
3
3
2
2
1
1
                           TABLE B538

    Organic Compounds Identified in Base Extract of Sample No. 177B
       Relative
Peak  Retention
No.      Time
Compound
Approximate
   Level
   (ppb)
 1     1.000

 2     2.589
Camphor

Diethyl Hexyl  Phthalate

-------
                              263
                          TABLE B539

       Volatile Organic Compounds Identified in Sample No. 178S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


 1     1.000       Chloroform                                   3
                           TABLE  B540

    Organic Compounds Identified in Acid Extract of Sample N0.178A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.522
0.595
0.667
0.731
0.796
0.858
Compound
C,Q Alcohol
C,, Alcohol
C,2 Alcohol
C13 Alcohol
C,. Alcohol
C,,- Alcohol
1 b
Approximate
Level
(ppb)
2
3
2
3
3
2

-------
                              264
                           TABLE B541
    Organic Compounds Identified in Base Extract of Sample No.1788


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1      1.000       Camphor  (IS)
  2      2.578       Diethyl  Hexyl Phthalate                      1
                           TABLE B542

        Volatile Organic Compounds  Identified in Sample N0.179S


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1     1.000       Chloroform                                   8
                           TABLE  B543

     Organic Compounds Identified in Acid Extract of Sample No.  179A


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1      0.408      Methyl-2-Ethyl Hexanoate (IS)

  2      1.000      Methyl Palmitate                             2
  3      1.105      Methyl Stearate                              1

-------
                               265
                           TABLE B544
    Organic Compounds Identified in Base Extract of Sample No.l79B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

 1     0.606       Dichlorobutane                               5
 2     1.000       Camphor (IS)
                           TABLE B545
        Volatile Organic Compounds  Identified in Sample No. 180S


        Relative                                             Approximate
 Peak   Retention                                               Level
 No.     Time       Compound   .                                (ppb)


  1      1.000       Chloroform                                   2

  2      1.065       1,2-Dichloroethane                           1

-------
                          266
                       TABLE  B546
Organic Compounds Identified  in Acid Extract of Sample No.lSOA

Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12

13
14
15

Relative
Retention
Time
0.426
0.742
0.804
0.862
0.920
0.978
1.000
1.031
1.086
1.108
1.135
1.181

1.227
1.273
1.353



Compound
Methyl -2-Ethyl Hexanoate (IS)
C,- Alcohol
C]4 Alcohol
C,5 Alcohol
C,c Alcohol
ID
C,7 Alcohol
Methyl Palmitate
C,0 Alcohol
its
C,g Alcohol
Methyl Stearate
C2Q Alcohol
C01 Alcohol
21
C22 Alcohol
C23 Alcohol
Diethyl Hexyl Phthalate
TABLE B547
Organic Compounds Identified in Base Extract of Sample

Peak
No.
1
2
3
Relative
Retention
Time
0.645
1.000
2.532


Compound
Dichlorobutane
Camphor (IS)
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
2
2
2
2
4
1
1
3
1
1

1
1
2

No. 1 SOB
Approximate
Level
(ppb)
3
—
1

-------
                               267
                           TABLE B548
        Volatile Organic Compounds  Identified  in  Sample  No. 181S

Peak
No.
1
2
Relative
Retention
Time
1.000
1.177


Compound
Chloroform
1 ,1 ,1-Trichloroethane
Approximate
Level
(ppb)
3
1
                           TABLE B549
     Organic  Compounds  Identified in Acid Extract of Sample No. 181A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.481
0.904
1.000
1.120
1.278
1.352
1.447
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,c Terpene
Methyl Palmitate
C,,- Terpene
Methyl Dehydroabietate
?
?
Approximate
Level
(ppb)
_ _ ..
1
3
2
1
1
1
                           TABLE B550
    Organic Compounds Identified in Base Extract of Sample No.lSIB

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound

  1      1.000       Camphor (IS)
  2      2.606       Diethyl  Hexyl Phthalate

-------
                              268
                          TABLE B551
       Volatile Organic Compounds Identified in Sample No.1825


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1     1.000       Chloroform                                   1

  2     1.783       Bromobenzene                                 3
                           TABLE B552

    Organic  Compounds  Identified in Acid Extract of Sample No. 182A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.426
1.000
1.089
1.095
1.102
1.230
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Dibutyl Phthalate
Methyl Stearate
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
5
4
3
6
11
2

-------
                          269
                       TABLE  B553
Organic Compounds Identified  in Base Extract of Sample  No.1826
Peak
No.
1
2
3


Peak
No.
1
2
3
4
5
6

Relative
Retention
Time
0.627
1.000
2.558

Volatile
Relative
Retention
Time
1.000
1.425
1.725
1.949
2.114
2.421

Compound
Dichlorobutane
Camphor (IS)
Diethyl Hexyl Phthalate
TABLE B554
Organic Compounds Identified in
Compound
Chloroform
1 ,2-Bromo-Chloroe thane
Dibromoethane
Methyl Ethyl Dioxolane
Tetrachl oroethyl ene
Acetophenone
TABLE B555
Organic Compounds Identified in Acid Extract
Peak
No.
1
2
3
4
Relative
Retention
Time
0.379
1.000
1.107
1.352
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
2
—
1

Sample No.l83S
Approximate
Level
(ppb)
1
2
4
1
1
1

of Sample No. 183A
Approximate
Level
(ppb)
—
3
2
1

-------
                          270
                       TABLE  B556
Organic Compounds Identified  in Base Extract  of Sample  No.1836
Peak
No.
1
2
3
4


Peak
No.
1
2
3

Relative
Retention
Time
0.473
1.000
2.105
2.585

Volatile
Relative
Retention
Time
0.879
1.000
2.146
/
Compound
Dichlorobutane
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
TABLE B557
Organic Compounds Identified in Sample No.
Compound
Tetrahydrofuran
Chloroform
Toluene
TABLE B558
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.305
0.416
1.000
1.108
1.235
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
?
Approximate
Level
(ppb)
4
—
1
2

184S
Approximate
Level
(ppb)
1
12
1

N0.184A
Approximate
Level
(ppb)
2
—
2
2
1

-------
                              271
                           TABLE B559

    Organic Compounds Identified in Base Extract of Sample No. 184B


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1      1.000      Camphor  (IS)

  2      2.689      Diethyl  Hexyl Phthalate                      1
                           TABLE B560

        Volatile Organic Compounds  Identified in Sample No. 185S
Peak
No.
1
2
Relative
Retention
Time
0.948
1.000
Compound
Diethyl Ether
Chloroform
Approximate
Level
(ppb)
4
11
                            TABLE  B561

     Organic  Compounds  Identified  in Acid  Extract of Sample N0.185A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.420
1.000
1.065
1.116
1.174
1.371
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Methyl Stearate
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
...
1
13
1
2
1

-------
                              272
                          TABLE B562
    Organic Compounds Identified  in  Base  Extract  of  Sample  No.  185B
Peak
No.
1
2
3
Relative
Retention
Time
0.542
1.000
2.607
Compound
Dichlorobutane
Camphor (IS)
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
3
—
1
                           TABLE  B563
       Volatile Organic Compounds Identified in Sample No. 186S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

                   No peaks over 1 PPB.
                           TABLE  B564
    Organic Compounds Identified  in  Acid  Extract  of Sample  N0.186A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.400
1.000
1.103
1.110
1.349
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Dibutyl Phthalate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
—
1
1
1
1

-------
                               273
                           TABLE B565

    Organic Compounds Identified in Base Extract of Sample No.1866


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


   1     0.557      Dichlorobutane                               9

   2     1.000      Camphor (IS)
                           TABLE B566
        Volatile Organic Compounds  Identified  in Sample No. 187S


       Relative                                            Approximate
 Peak   Retention                                               Level
 No.     Time       Compound                                   (ppb)


   1     1.000      Chloroform                                   3

   2     2.239      Toluene                                      1
                           TABLE B567
    Organic Compounds Identified in Acid Extract of Sample N0.187A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


                   No peaks over 1 PPB.

-------
                               274
                           TABLE B568
    Organic Compounds Identified in Base Extract of Sample No.1876

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)


                   No peaks over 1 PPB.
                           TABLE B569
        Volatile Organic Compounds  Identified in Sample No. 188S
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
1.000
1.157
1.414
1.452
.1.959
2.029
Compound
Chloroform
1 ,1 ,1-Trichloroethane
Dimethyl Disulfide
Trichloroethylene
Tetrachl oroethyl ene
Toluene
Approximate
Level
(ppb)
2
4
1
3
13
2

-------
                          275
                       TABLE B570
Organic Compounds Identified in Acid  Extract  of  Sample  No.lSSA
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Relative
Retention
Time
0.411
0.487
0.521
0.554
0.591
0.621
0.654
0.688
0.751
0.775
0.806
0.815
0.873
0.887
0.918
0.933
0.945
0.988
1.000
1.021
1.042
1.058
1.073
1.109
1.142
1.160
1.182
1.203
1.212
1.224
1.239
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
Hydrocarbon C > 8
Hydrocarbon C > 8
Hydrocarbon C > 10
Hydrocarbon C > 10
Hydrocarbon C > 10
Hydrocarbon C > 10
Hydrocarbon C >_ 12
Hydrocarbon C >_ 12
Hydrocarbon C >_ 12
Tetrachloroanisole
Hydrocarbon C >_ 14
Methyl Myri state
Methyl Naphthoate
Hydrocarbon C >_ 16
Pentachloroanisole
Hydrocarbon C >_ 16
Methyl Palmitate
?
Hydrocarbon C >_ 18
?
?
Methyl Stearate
?
?
Methoxy Carbonyl Benzophenone
?
C16H10
?
?
Approximate
Level
(ppb)
—
1
1
1
1
1
1
4
6
4
8
10
17
10
3
12
14
1
30
5
17
20
5
87
23
17
27
35
2
37
35

-------
                          276
                    TABLE B570, cont.
Organic Compounds Identified in Acid Extract of Sample  No.lSSA (continued)
Peak
No.
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
Relative
Retention
Time
1.269
1.279
1.318
1.330
1.351
1.360
1.369
1.388
1.400
1.409
1.418
1.427
1.446
1.457
1.482
1.497
1.536
1.558
1.567
1 . 582
Compound
7
?
?
Fatty Acid Methyl Ester C >_ 20
Di ethyl Hexyl Phthalate
?
Fatty Acid Methyl Ester C >_ 24
?
Hydrocarbon C >_ 28
?
?
?
7
7
7
7
7
7
7
7
Approximate
Level
(ppb)
15
82
18
3
31
80
39
20
10
35
40
31
45
27
42
9
33
10
27
12

-------
                          277
                       TABLE B571
Organic Compounds Identified in Base Extract  of Sample  No.l88B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
Relative
Retention
Time
1.000
1.049
1.146
1.214
1.287
'1.317
1.348
1.378
1.438
1.470
1.531
1.592
1.732
1.787
1.806
2.007
2.032
2.147
2.184
2.221
2.276
2.312
2.349
2.373
2.416
2.440
2.465
2.489
2.550
2.574
Compound
Camphor (IS)
?
?
Hydrocarbon C >_ 12
Methyl Naphthalene
Methyl Naphthalene
Hydrocarbon C >_ 12
Indole
Dimethyl Naphthalene
Dimethyl Naphthalene
?
Biphenyl
Methyl Acenaphthene
Diethyl Phthalate
7
Phenanthrene
Diisobutyl Phthalate
?
Dibutyl Phthalate
Caffeine
Hydrocarbon. C >_ 20
Hydrocarbon C >_ 20
C16H10
Hydrocarbon C ^ 22
C16H10
Hydrocarbon C ^ 22
Hydrocarbon C >_ 22
Hydrocarbon C >_ 22
Hydrocarbon C >_ 24
Hydrocarbon C >_ 24
Approximate
Level
(ppb)
—
3
2
1
1
1
3
11
3
3
3
2
2
2
1
1
2
4
8
6
5
1
1
1
1
1
1
1
2
1

-------
                              278
                        TABLE  B571,  cont.
    Organic Compounds Identified in  Base Extract of Sample  No.1886  (continued)
Peak
No.
31
32
33
34
35
36
37
38
39
Relative
Retention
Time
2.636
2.691
2.709
2.752
2.825
2.910
2.989
3.069
3.173
Compound
Hydrocarbon C > 24
Diethyl Hexyl Phthalate
Hydrocarbon C >_ 26
Hydrocarbon C ^ 26
C,,- Terpineol
?
?
?
?
Approximate
Level
(ppb)
2
4
1
1
4
3
3
10
13
                           TABLE B572
       Volatile Organic Compounds Identified in Sample No. 189S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1      1.000      Chloroform                                   1

-------
                               279
                            TABLE  B573
    Organic  Compounds  Identified  in Acid Extract of Sample N0.189A


       Relative                                            Approximate
Peak  Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1       0.400       Methyl-2-Ethyl  Hexanoate  (IS)

  2       1.000       Methyl  Palmitate                              1
  3       1.342       Diethyl  Hexyl  Phthalate                       1
                            TABLE B574
     Organic Compounds Identified in Base Extract of Sample No.1896


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


   1      1.000      Camphor (IS)

   2      2.692      Diethyl Hexyl Phthalate                      1

-------
                       280
                    TABLE B575
Volatile Organic Compounds Identified in  Sample  No.190S
Peak
No.
1
2
3
4
5
6
7
8

Relative
Retention
Time
0.412
0.956
1.000
1.544
1.619
1.882
2.194
2.282

Compound
t
Acetone
Diethyl Ether
Chloroform
?
Benzene
Bromobenzene
Tetrachloroethylene
Toluene
TABLE B576
Organic Compounds Identified in Acid Extract of Sample
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Relative
Retention
Time
0.356
0.684
0.753
0.798
0.809
0.944
1.000
1.062
1.098
1.104
1.113
1.234
1.278
1.375
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
?
Methyl -2-(4-chlprophenoxy) Butanoate
Tetrachloroanisole
Pentachl oroani sol e
Methyl Palmitate
?
Di butyl Phthalate
Methyl Stearate
Caffeine
?
?
?
Approximate
Level
(ppb)
3
1
3
2
4
8
1
1

N0.190A
Approximate
Level
(ppb)
—
1
1
2
1
1
2
5
2
5
3
15
. 5
8

-------
                               281
                           TABLE B577

     Organic  Compounds  Identified in Base Extract of Sample No.1908
Peak
No.
1
2
3
4
5
6
7
8
9
Relative
Retention
Time
1.000
1.856
2.284
2.317
2.389
2.422
2.759
2.837
3.133
Compound
Camphor (IS)
?
Dibutyl Phthalate
Caffeine
Hydrocarbon C >_ 20
?
?
Di ethyl Hexyl Phthalate
?
Approximate
Level
(ppb)
—
1
2
4
1
1
6
3
1
                            TABLE  B578

       Volatile Organic Compounds  Identified in Sample No.  191S


       Relative                                             Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       0.490      Acetone                                       2

  2       1.110      Methyl Ethyl Ketone                         23

  3       2.274      Benzaldehyde                                  1

-------
                          282
                       TABLE  B579
Organic Compounds Identified  in Acid  Extract  of  Sample  No. 191A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
Relative
Retention
Time
0.400
0.804
0.817
0.872
0.887
0.933
0.948
0.982
1.000
1.033
1.040
1.055
1.064
1.107
1.143
1.159
1.180
1.204
1.216
1.235 .
1.284
1.293
1.353
1.378
1.506
1.595
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl -2- (4-chlorophenoxy) Butanoate
Tetrachloroanisole
Hydrocarbon C > 14
Methyl Myri state
Hydrocarbon C >_ 16
Pentachloroanisole
Fatty Acid Methyl Ester C >_ 15
Methyl Palmitate
?
Fatty Acid Methyl Ester C >_ 16
Fatty Acid Methyl Ester C >_ 17
?
Methyl Stearate
Fatty Acid Methyl Ester C >_ 18
Fatty Acid Methyl Ester C >_ 18
?
Fatty Acid Methyl Ester C >_ 20
?
?
?
Fatty Acid Methyl Ester C >_ 22
Diethyl Hexyl Phthalate
?
?
7
Approximate
Level
(ppb)
—
12
14
21
30
33
24
5
252
25
45
49
13
425
34
48
32
70
8
95
40
66
34
57
53
79

-------
                          283
                       TABLE B580
Organic Compounds Identified in Base  Extract  of  Sample  No.191B
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
Relative
Retention
Time
0.549
1.000
1.181
1.310
1.421
1.473
1.532
1.549
1.661
1.729
1.755
1.748
1.819
1.877
2.029
2.088
2.182
2.217
2.270
2.339
2.469
2.515
2.586
2.703
Compound
Dichlorobutane
Camphor (IS)
Hydrocarbon C > 10
Hydrocarbon C > 12
Hydrocarbon C > 12
Hydrocarbon C > 12
Hydrocarbon C > 14
Hydrocarbon C > 14
Hydrocarbon C > 14
?
Hydrocarbon C > 16
Hydrocarbon C >_ 16
Hydrocarbon C > 16
Hydrocarbon C > 16
Hydrocarbon C > 18
Dibutyl Phthalate
Hydrocarbon C 20
Hydrocarbon C 20
?
Hydrocarbon C 22
Hydrocarbon C 24
Hydrocarbon C 24
Diethyl Hexyl Phthalate
C,r Terpineol
Approximate
Level
(ppb)
3
—
1
1
1
1
3
3
18
13
12
15
20
59
59
60
38
48
123
41
18
20
58
35

-------
                        284
                    TABLE B581
Volatile Organic Compounds Identified in Sample  No.1925
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
No peaks over 1 PPB.


TABLE B582
Organic Compounds Identified in Acid Extract of
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.400
0.602
0.672
0.738
0.801
0.861
0.921
0.979
1.000
1.030 .
1.084
1.099
1.105
1.129
1.181
1.226
1.271
1.287
1.310
1.352
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,, Alcohol
C12 Alcohol
C,3 Alcohol
C,. Alcohol
C15 Alcohol
Cnc Alcohol
1 0
C,7 Alcohol
Methyl Palmitate
CIQ Alcohol
C,g Alcohol
Di butyl Phthalate
Methyl Stearate
C2Q Alcohol
C2-, Alcohol
C22 Alcohol
C23 Alcohol
Butyl Phthalyl Butyl Glycolate
C24 Alcohol
Diethyl Hexyl Phthalate

Sample No. 192A
Approximate
Level
(ppb)
—
5
7
9
12
15
13
5
5
4
2
2
3
2
2
1
1
1
1
2

-------
                               285
                           TABLE B583

    Organic Compounds Identified in Base Extract of Sample No.  192B
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.645
1.000
2.076
2.437
2.553
Compound
Dichlorobutane
Camphor (IS)
Di butyl Phthalate
Butyl Phthalyl Butyl Glycolate
Di ethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
—
2
1
3
                            TABLE  B584

       Volatile Organic Compounds Identified in Sample N0.193S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks  over  1  PPB.

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                               286
                           TABLE B585
    Organic Compounds Identified in Acid Extract of Sample N0.193A
Peak
No.
1
2
3
4
5
Relative
Retention
Time
0.430
1.000
1.096
1.102
1.346
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Di butyl Phthalate
Methyl Stearate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
— _
1
1
1
1
                            TABLE  B586
     Organic Compounds  Identified  in  Base  Extract of Sample No.1936
Peak
No.
1
2
3
4
Relative
Retention
Time
0.570
1.000
2.106
2.595
Compound
Dichlorobutane
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
4
—
1
1
                            TABLE  B587
       Volatile Organic Compounds Identified in Sample No.l94S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

                   No  peaks  over  1  PPB.

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                          287
                       TABLE B588
Organic Compounds Identified in Acid  Extract  of  Sample  N0.194A
Peak
No.
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Relative
Retention
Time
0.370
0.442
0.504
0.561
0.623
0.685
0.847
0.807
0.866
0.923
0.979
1.000
1.032
1.083
1.100
1.105
1.130
1.175
1.219
1.343
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Cg Alcohol
C-JQ Alcohol
C,, Alcohol
C12 Alcohol
C,3 Alcohol
C]4 Alcohol
C,r Alcohol
1 D
C,c Alcohol
1 b
C,7 Alcohol
Methyl Palmitate
C,g Alcohol
C,g Alcohol
Dibutyl Phthalate
Methyl Stearate
C2Q Alcohol
C2, Alcohol
C22 Alcohol
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
1
—
3
2
2
3
3
2
1
1
1
2
1
1
1
1
1
1
1
1

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                              288
                           TABLE B589

    Organic Compounds Identified in Base Extract of Sample No.1946

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


   1      1.000      Camphor (IS)
   2      2.789      Diethyl Hexyl Phthalate                      2
                            TABLE B590
       Volatile Organic Compounds  Identified  in Sample No.1955


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks  over 1  PPB.

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                               289
                           TABLE B591
    Organic Compounds  Identified in  Acid  Extract  of  Sample  N0.195A
Peak
No.
1
2
3
4
5
6
7
Relative
Retention
Time
0.410
1.000
1.064
1.097
1.107
1.238
1.351
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
?
Dibutyl Phthalate
Methyl Stearate
?
Diethyl Hexyl Phthalate
Approximate
Level
(ppb)
-. _ _
4
2
1
2
2
1
                           TABLE B592
    Organic Compounds Identified in Base Extract of Sample No.l95B

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time       Compound                                   (ppb)

   1      0.642      Dichlorobutane                               3
   2      1.000      Camphor (IS)
   3      2.499      Diethyl Hexyl Phthalate                      4

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                               290
                            TABLE B593
       Volatile Organic Compounds Identified in Sample No.1965


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks  over 1  PPB.
                            TABLE B594

     Organic  Compounds  Identified  in Acid Extract of Sample N0.196A

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


  1       0.410      Methyl-2-Ethyl  Hexanoate  (IS)

  2       1.000      Methyl  Palmitate                              1

  3       1.105      Methyl  Stearate                              1
                            TABLE B595
     Organic Compounds  Identified  in  Base  Extract  of  Sample N0.196B

       Relative                                            Approximate
Peak   Retention                                                Level
 No.      Time       Compound                                    (ppb)


   1      0.666      Dichlorobutane                               6
   2      1.000      Camphor (IS)
   3      2.462      ?                                            1

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                               291
                            TABLE B596
       Volatile Organic Compounds Identified in Sample N0.197S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No peaks over 1 PPB.
                            TABLE B597

     Organic  Compounds  Identified  in Acid Extract of Sample N0.197A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.352
0.430
1.000
1.102
Compound
1 ,1 ,2,2-Tetrachloroethane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
1
—
3
3
                            TABLE B598

     Organic Compounds Identified in Base Extract of Sample  No.1978

        Relative                                             Approximate
 Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


   1     0.637      Dichlorobutane                               7

   2     1.000      Camphor (IS)
   3     2.451      ?                                            2

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                               292
                            TABLE B599
       Volatile Organic Compounds Identified in Sample No.1985


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks over  1  PPB.
                            TABLE B600
    Organic Compounds Identified in Acid Extract of Sample N0.198A

Peak
No.
1
2
3
4
Relative
Retention
Time
0.919
1.976
1.000
1.027


Compound
C,c Alcohol
1 0
C,7 Alcohol
Methyl Palmitate
C-,a Alcohol
Approximate
Level
(ppb)
1
1
1
1
                            TABLE B601

     Organic  Compounds  Identified  in Base Extract of Sample No.1986

       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No  peaks  over  1 PPB.

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                               293
                            TABLE B602
       Volatile Organic Compounds Identified in Sample No.1995

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

  1       0.502      Butadiene                                    2
  2       1.000      Chloroform                                   1
                            TABLE B603
    Organic Compounds  Identified in Acid Extract of Sample N0.199A
Peak
No.
1
2
3
Relative
Retention
Time
0.420
1.000
1.104
Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
___
2
1
                            TABLE B604
     Organic Compounds Identified in Base Extract of Sample  No.1996
Peak
No.
1
2
Relative
Retention
Time
0.656
1.000
Compound
Dichlorobutane
Camphor (IS)
Approximate
Level
(ppb)
4
—

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                               294
                            TABLE B605
       Volatile Organic Compounds Identified in Sample No.200S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks over  1  PPB.
                            TABLE B606

     Organic  Compounds  Identified  in Acid  Extract of Sample No.200A
Peak
No.
1
2
3
4
Relative
Retention
Time
0.280
0.362
0.431
1.000
Compound
Dichlorobutane
Dichlorobutane
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Approximate
Level
(ppb)
1
1
—
1
                             TABLE  B607

     Organic Compounds Identified in Base Extract of Sample No. 200B


        Relative                                            Approximate
 Peak  Retention                                               Level
 No.      Time      Compound                                   (ppb)


    1     0.653      Dichlorobutane                               7
    2     1.000      Camphor  (IS)

-------
                               295
                            TABLE B608
       Volatile Organic Compounds Identified in Sample No.201S

       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)

                   No  peaks over  1 PPB.
                            TABLE B609
     Organic  Compounds  Identified  in Acid  Extract of Sample N0.201A
Peak
No.
1
2
3
4
5
6
Relative
Retention
Time
0.396
0.758
0.804
0.891
1.000
1.103
Compound
Methyl -2-Ethyl Hexanoate (IS)
?
C 14 Alcohol
Methyl Myristate
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
—
1
1
2
2
2

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                               296
                            TABLE B610

     Organic  Compounds  Identified  in  Base  Extract of Sample No.2016


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


   1      0.659      Dichlorobutane                               1

   2      1.000      Camphor (IS)

   3      2.481       Diethyl Hexyl  Phthalate                      1
                             TABLE B611
       Volatile Organic Compounds  Identified in Sample No.202S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks  over 1  PPB.
                             TABLE .8612
     Organic Compounds Identified in Acid Extract of Sample  No.202A


       Relative                                             Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


                    No peaks over 1  PPB.

-------
                                297
                             TABLE  B613
     Organic Compounds  Identified in  Base  Extract of Sample No.202B


       Relative                                            Approximate
Peak   Retention                                               Level
 No.      Time       Compound                                   (ppb)


   1      0.644      Dichlorobutane                                3

   2      1.000      Camphor (IS)
                             TABLE  B614
       Volatile Organic Compounds  Identified in Sample No.203S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


  1       1.000      Chloroform                                   4
                             TABLE B615
     Organic  Compounds  Identified  in Acid Extract of Sample No.203A

Peak
No.
1
2
3
Relative
Retention
Time
0.443
1.000
1.096


Compound
Methyl -2-Ethyl Hexanoate (IS)
Methyl Palmitate
Methyl Stearate
Approximate
Level
(ppb)
	
1
1

-------
                                298
                             TABLE  B616

    Organic Compounds  Identified in Base Extract of Sample No.2036


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


   1     0.631      Dichlorobutane                               5

   2     1.000      Camphor  (IS)

   3     2.409      Butyl  Phthalyl  Butyl Glycolate               3
                             TABLE B617
       Volatile Organic Compounds  Identified in Sample No.204S


       Relative                                            Approximate
Peak  Retention                                               Level
No.      Time      Compound                                   (ppb)


                   No  peaks  over  1  PPB.
                             TABLE B618
     Organic  Compounds Identified  in  Acid  Extract  of  Sample  No. 204A
Peak
No.
1
2
3
Relative
Retention
Time
0.420
0.815
1.000
Compound
Methyl -2-Ethyl Hexanoate (IS)
C,Q Terpineol
Methyl Palmitate
Approximate
Level
(ppb)
— — _
1
1

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                           299
                        TABLE B619
Organic Compounds Identified in  Base  Extract  of Sample  No.204B

Peak
No.
1
2
3
4
Relative
Retention
Time
0.639
1.000
1.532
2.412


Compound
Dichlorobutane
Camphor (IS)
C,Q Terpineol
?
Approximate
Level
(ppb)
3
—
3
1

-------