&EPA
United States
Environmental Protection
Agencv
EPA-600/7-86-Ol3b
April 1986
Research and
Development
ENVIRONMENTAL ASSESSMENT OF AN
ENHANCED OIL RECOVERY STEAM
GENERATOR EQUIPPED WITH AN EPA
HEAVY OIL LOW-NOx BURNER
Volume II. Data Supplement
Prepared for
Office of Air Quality Planning and Standards
Prepared by
Air and Energy Engineering Research
Laboratory
Research Triangle Park NC 27711
-------
RESEARCH REPORTING SERIES
Research reports of the Office of Research and Development, U.S. Environmental
Protection Agency, have been grouped into nine series. These nine broad cate-
gories were established to facilitate further development and application of en-
vironmental technology. Elimination of traditional grouping was consciously
planned to foster technology transfer and a maximum interface in related fields.
The nine series are:
1. Environmental Health Effects Research
2. Environmental Protection Technology
3. Ecological Research
4. Environmental Monitoring
5. Socioeconomic Environmental Studies
6. Scientific and Technical Assessment Reports (STAR)
7. Interagency Energy-Environment Research and Development
8. "Special" Reports
9. Miscellaneous Reports
This report has been assigned to the INTERAGENCY ENERGY-ENVIRONMENT
RESEARCH AND DEVELOPMENT series. Reports in this series result from the
effort funded under the 17-agency Federal Energy/Environment Research and
Development Program. These studies relate to EPA's mission to protect the public
health and welfare from adverse effects of pollutants associated with energy sys-
tems. The goal of the Program is to assure the rapid development of domestic
energy supplies in an environmentally-compatible manner by providing the nec-
essary environmental data and control technology. Investigations include analy-
ses of the transport of energy-related pollutants and their health and ecological
effects; assessments of, and development of, control technologies for energy
systems; and integrated assessments of a wide range of energy-related environ-
mental issues.
EPA REVIEW NOTICE
This report has been reviewed by the participating Federal Agencies, and approved
for publication. Approval does not signify that the contents necessarily reflect
the views and policies of the Government, nor does mention of trade names or
commercial products constitute endorsement or recommendation for use.
This document is available to the public through the National Technical Informa-
tion .Service. Springfield, Virginia 22161.
-------
EPA-600/7-86-013b
April 1986
ENVIRONMENTAL ASSESSMENT OF AN
ENHANCED OIL RECOVERY STEAM GENERATOR
EQUIPPED WITH AN EPA HEAVY OIL LOH-MOX BURNER
Volume II
Data Supplement
by
C. Castald1n1, L. R. Waterland, and R. DeRosler
Acurex Corporation
Energy & Environmental Division
555 Clyde Avenue
P.O. Box 7555
Mountain View, California 94039
EPA Contract 68-02-3188
EPA Project Officer: J. A. McSorley
Air and Energy Engineering Research Laboratory
Research Triangle Park, North Carolina 27711
For
U.S. ENVIRONMENTAL PROTECTION AGENCY
Office of Research and Development
Washington, DC 20460
-------
ABSTRACT
Comprehensive emission measurements and 30-day flue gas moni-
toring were performed on a 16-MW (55 million Btu/hr) enhanced oil re-
covery steam generator equipped with the EPA low-NOx burner firing
high-nitrogen crude. The 1-day comprehensive measurements included
quantification of semivolatile organics and 73 trace elements; volatile
organic sampling train (YOST) quantisation of volatile organic priority
pollutants; EPA Method 5/8 for particulate and SOX; controlled conden-
sation for SOx; Andersen imp actors for particle size distribution; grab
samples for N2O; and continuous flue gas monitoring. NOX emissions
during the comprehensive tests averaged 70 ppm at 3 percent O2, well
below the target level of 85 ppm. CO emissions were below 30 ppm, and
SO2 averaged about 550 ppm. Solid participates were emitted at about
27 ng/J (96 mg/dscm); condensible participates were about half that
level. Volatile organics (benzene, toluene, and ethylbenzene) were mea-
sured in the 0.4 to 20 ppb range. Semivolatile organics (naphthalene
and phenol) were detected in the 0.3 ppb range. Subsequent continuous
monitoring of flue gas criteria emissions showed NOX below 80 ppm at
3 percent G£ with an average of 70 ppm. CO emissions were generally
less than 30 ppm.
11
-------
CONTENTS
1 Introduction 1-1
2 Preliminary Tests and Equipment Calibration 2-1
3 Steam Generator Operating Data 3-1
4 Sampling Data Sheets 4-1
4.1 Continuous Monitoring Data 4-2
4.2 Field Data Sheets for EPA Method 5/8,
SASS, VOST, Andersen Impactor, Controlled
Condensation (CCS), and EPA Method 7 4-65
5 Analytical Results 5-1
5.1 Fuel Proximate and Ultimate Analyses 5-2
5.2 Particulate and Sulfur Oxides Emissions from
Method 5/8 Samples 5-4
5.3 Particulate Emissions from SASS Samples 5-12
5.4 Particulate Emissions Size Distributions from
Andersen Samples 5-17
5.5 Sulfur Oxides Emissions from Controlled
Condensation System Samples 5-26
5.6 Trace Element Analyses of Fuel and SASS Samples . . 5-30
5.7 Organic Analyses of SASS Samples: Total
Chromatographable Organics (TCO), Gravimetric
Organics (GRAY), Gas Chromatography Mass
Spectrometry (GC/MS), and Infrared (IR) Spectra of
Total Sample Extracts 5-44
5.8 Volatile Organics Analyses of VOST Traps 5-53
5.9 N20 Emissions by GC/ECD 5-59
5.10 NOX Emissions by EPA Method 7 5-61
-------
SECTION 1
INTRODUCTION
The purpose of this data supplement is to document test data in greater
detail than was possible in Volume I (Technical Results) of this report. It
is intended to provide sufficient detail for researchers to perform their own
analysis of the data obtained. Readers are referred to the technical volume
(Volume I) for objectives, description of the source tested, data
interpretations, and conclusions.
The remaining sections of this data supplement contain the following
information:
Section 2: Preliminary Tests and Equipment Calibration Stack
!
velocity traverse and nozzle .sizing and flow calculations;
equipment calibration data
Section 3: Steam Generator Operating Data Field data sheets of
steamer operating conditions from available test meters
Section 4: Sampling Data Sheets Emission data obtained with
continuous monitoring instrumentation. Operating data
tables for combined EPA Methods 5/8 (for particulate mass
and SOX emissions), source assessment sampling system (SASS)
(for trace element and organic emissions), volatile organic
sampling train (VOST) (for volatile organic species
emissions), Andersen impactor (for particulate size
1-1
-------
distribution), controlled condensation system (for $62,
$03), and EPA Method 7 (for NOX certification)
Section 5: Analytical Results Fuel proximate and ultimate analyses;
laboratory reports for particulate emissions and size
distribution by gravimetric analyses; sulfur oxides
emissions by wet chemical analysis; trace element analyses
by spark source mass spectrometry (SSMS); atomic absorption
spectroscopy (AAS) and other methods; total
chromatographable organic (TCO) and gravimetric organic
(6RAV) results, determination of organic compounds by gas
chromatography/mass spectrometry (GC/MS) and infrared (IR)
spectra of GRAY residues, volatile organics analyses of YOST
traps by GC/MS; NgO analysis by GC/electron capture detector
(ECD); and laboratory analyses for NOX by EPA Method 7.
1-2
-------
SECTION 2
PRELIMINARY TESTS AND EQUIPMENT CALIBRATION
2-1
-------
PRELIMINARY VELOCITY TRAVERSE
?l fliiy -- .' -':-", >.__ _
IUTF - - - *' -
nraTinN " /.-^'^,
n-ArK in 1- .
BAROMETRIC PRESS
STACK GAUGE PRES
HBP in Hp .5/^ --^V
5IIRF > H.O
'. 4~
TRAVERSE
POINT
NUMBER
/
.-L
-?
^,
*
x
-*
/
K
AVERAGE
VELOCITY
HEAD
(ips),in.H20
-,-1
v ^ '-T
^:
1 "7
^ '<
i
* - s^*
__/j
. -- -"i'
. ^'i-
/ / x
STACK
TEMPERATURE
(Ts), *F
// / ^*
s/:{
;,"- '/
Ox. .
^ -5
"" >' ' 1
~ .7-7
-/^^
- .' X
^ ^ .-'
V T :/
SCHEMATIC OF TRAVERSE POINT LAYOUT
EPA (Dur) 233
2-2
TRAVERSE
POINT
NUMBER
;
-^
^
s
^
-1
<
'7
J
"i
AVERAGE
VELOCITY
HEAD
(Aps), in.H20
"V .- ;
. 1 ' ^
,^ .5 1
,«^-3
,-fe
7*-"^
,C :^'
,'''Tt^^>
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llr-ix
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STACK
TEMPERATURE
^- y y f f . /
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--.^
I ]
1 .'
J /
. . . .... .. . '_'.-.::X>
-------
Plant,
Date
ISOKINECTIC SAMPLING WORKSHEET
j Peformed by
Sample Location_
Test No./Type
K = 782.687 (Cp)2 (1-BWO)2 Ps Md
Ms Pm
where: K = Contant of fixed and assumed parameters (dimensionless)
Pitot coefficient (dimensionless)
Water vapor in the gas stream
(proportion by volume)
"Absolute stack gas pressure (in. Hg)
Molecular weight, stack gas dry
(Ib/lb-mole)
Orifice coefficient (dimensionless)
Molecular weight, stack gas wet
(Ib/lb-mble) Md(l-Bwo) + 18(BWQ)
Abolute meter pressure (in. Hg)
782.687 (.-.V^Z (1-j )2 (2*. :Q (^ y
(^L)2 (-iL£) (-£11)
CP
Bwo
PS
"d
KO
Ms
Pm
K
-" .^
. //
-/. 3/
>". C* '
!)-' ~J<_7
'. s ' '
^^o
.2 y;-= v
-:r_Ni. J-C
2-3
-------
P1 ant Cjf-o-.KCyA.
Date sJ i /V-H-
ISOKINECTIC SAMPLING WORKSHEET
Peformed by
Sample Location
Test No./Type 1-P5& -'
K = 782.687 (Cp)2 (1-BWO)2 Ps Md
Ms Pm
where: K = Contant of fixed and assumed parameters (dimensionless)
Pitot coefficient (dimensionless)
Water vapor in the gas stream
(proportion by volume)
Absolute stack gas pressure (in. Hg)
Molecular weight, stack gas dry
(Ib/lb-mole)
Orifice coefficient (dimensionless)
Molecular weight, stack gas wet
(Ib/lb-mole) Md(l-BwQ) + 18(BWQ)
Abo lute meter pressure (in. Hg)
782.687 ( )2 (1- )2 ( ) ( )
( )2 ( ) ( )
CP
BWO
PS
"d
KO
3L
Ms
Pm
K
,5lfe
f\ i !
^
.'^T^Tt'v ^^
C!^~. (4
V-VjS. l~
Cs-'S
h-L-fS
? %
-------
Plant
Date a.
Sample Location_
Test No./Type S
ISOKINECTIC NOZZLE CALCULATION
AND
SAMPLING RATE CALCULATION
Performed by_
*H
25
where: N
-------
ACUREX
Corporation
ANDERSEN SAMPLING CALCULATIONS
Plant
5 rj ~ 6 7
Test Location
Pitot Coefficient (Cp)
Duct Dimension
Barometric Pressure (PQ)
Static Pressure (Pst)
Meter Temp (Tm)
Meter Rate (Rm)
Clock Time
" Hg
" H2O
°F
cfm
1) Stack Pressure: PS = Pb * =
jn. Hg.
2) Mole Fraction Dry Gas: Mf 1 -
100 = 1 " 100
3) Mol. Wt. Dry Flue Gas:
MWd (0.44 x %CO2) + (0.32 x %O2) + (0.28 x %CO) + (0.28 x %N2)
- (0.44 x /* & ) + (0.32 x ai.3* ) + (0.28 x ) + (0.28 x
4) Mol. Wt. Flue Gas:
MWS (MWd) x (Mf) + [18 x (1 Mf)]
= 5*3*
[18 x
5) Stack Gas Velocity:
V = 85.49 x (Cp) X /Zp avg x / s-±-^°-.
V V Ps x MWs
85.49 X
.X
460 =
6) Sample Rate:
Qn 0.327 x (Vs) x
= 0.327 x '
gcfm
7) Meter Rate:
Form EED-070A 12/79
-------
CONTROL MODULE CALIBRATION
Module I.D.
Date //)-ST- S3
Barometric Pressure (In. Hg) 30* Of
Primary Meter I.D.
Ambient Temperature (°F)
Operator
Orifice
Size
Orifice
Reading
AH
(In H20)
Primary Meter
Gas Volume
VP
(ft3)
Meter Box
Gas Volume
,
(ft3)
Temperature
Primary Meter
Inlet
Tpl C
Outlet
Average
Tp CF)
Meter Box Meter
Inlet
Outlet
Tdo (°F)
Average
Td (°F)
Time
0
(mln)
Meter
Correction
Factor
Orifice
Coefficient
"o
Small
Orifice
0.187
I 7/0
_2L
J-0
JU.IK
JLISS
JZtfO
SM
JI.M
7f.3
/.OOP
^5:7
LOO 3
?V
I.06.B
,&TL
re
Medium
Orifice
0.261
-tiffs'
J.O
30. faO
J. 010
75IJ
Wf
77.3
I.Q/f
77. S"
//.i
/.77I
U1I
Large
Orifice
0.358
.to
jLo
33.
31. 3/0
V.o
73.5^00
~3M.
.OO.S
/OS
~ML
Ml
3.671.
J.J3!
« Vd (PB * AH \ (T +
V TJ7S/ v
/AH (TH +
0-v/ PU (28.
460)
9B1~^
Orifice
Small
Medium
Large
Avg. a
/.oot
AO/Z
Avg. K0
-------
SECTION 3
STEAM GENERATOR OPERATING DATA
3-1
-------
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7. /--.<-
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-------
SECTION 4
SAMPLING DATA SHEETS
4.1 Continuous Monitoring Data
4.2 Field Data Sheets for EPA Method 5/8, SASS, YOST, Andersen Impactor,
Controlled Condensation (CCS), and EPA Method 7
4-1
-------
4.1 CONTINUOUS MONITORING DATA
4-2
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant
Location.
Operator.
Date
Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
F.ial X./^-' :.'/.':,
Time
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%
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Total
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Non-
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HC
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Temp
F
COMMENTS
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AVERAGE
t
co
032 I /82
-------
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HYDROCARBONS (HCl
Total
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Non-
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S
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F
COMMENTS
AVERAGE
032
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Planl C.M&*K(MV ! ££f- )
Location,
Operator
Hate
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Tim*
<5o3o
O/&O
<9«}30
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HC
S
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Temp
F
COMMENTS
AVERAGE
I /82
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant
Location.
Operator-
Load Range.
1
Ambient Temperature
Barometric Pressure
Static Pressure Duct
Time
Sampte
Point
Load
MW
Sloam
Flow
Ib/hr
KtOOO
DRY UNCORRECTEO
CO
ppm
ppm
NO
ppm
CORRECTED TO
3*i OZ DRY
HYDROCARBONS (HC|
NOM
ppm
NO2
ppmn
NO
ppm
NO,
PPm
N02
ppm
Total
HC
Molhano
Non-
Methane
HC
Slack
Gas
Temp
F
COMMENTS
r/
JS
f
a
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jfCL
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3-7
A'"
i & 5
AV.'
Staff
3-3
,*
3-3
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3-3
9c.>
AVERAGE
30
032 1/82
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant
Location _
Operator.
Date
\
Load Range-
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
Time
/8SZ
/4o8
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J ?:l£
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Point
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MW
r\-
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Steam
Flow
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DRY UNCORRECTED
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ppmn
CORRECTED TO
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ppm
N0x
ppm
NO,
ppm
HYDROCARBONS (HC)
Tolal
HC
Methane
Non-
Melhane
HC
b
Slack
Gas
Temp
F
COMMENTS
AVERAGE
032 1/82
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant fto&torf (.£**.)
Locatior
Operato
Dflto
Load Ra
Time
/0tf f
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-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant (.rtZVAotJ i ££*. 1
Location
Operator
DfttA
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Time
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Barometric Pressure _
Static Pressure Duct
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Point
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MW
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FIELD DATA SHEET
Aerotherm
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Location.
Date.
Ambient Temperature
Barometric Pressure _
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Date
Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct_
Fuel
\
Tim*
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Point
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Plant
Location.
Operator.
Date_
Load Range-
Ambient Temperature
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Static Pressure Duct _
Fuel
Time
Sample
Point
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MW
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032 |/82
-------
FIELD DATA SHEET
ACUREX
Aerotherm
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Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
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Load Range.
Time
SimpM
Poml
Lo«i
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Location.
V
Operator.
Date
Load Range
Ambient Temperature.
Barometric Pressure _
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Fuel
Tim.
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MW
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032 1/82
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FIELD DATA SHEET
ACUREX
Aerotherm
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Location _
Operator.
Date
Load Range-
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct_
Fuel
Time
Sample
Point
Load
MW
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Flow
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Location.
Operator.
Date
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Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
S3 C
Time
SimpM
Point
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Slum
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Date.
Load Range.
Ambient Temperature.
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*
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Fuel
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Location.
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Operator.
Date
Load Range-
Ambient Temperature
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Static Pressure Duct
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Time
Sample
Point
Load
MW
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Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
Tim*
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Location.
Operator.
Date
Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
TlIM
SwnpM
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tow!
MW
SlMm
Flow
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FIELD DATA SHEET
ACUREX
Aerotherm
Plant
Location.
Operator.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Load Range-
TlIM
Sample
Point
MW
Slum
Flow
Ib/hr
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CO
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so
NO
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ppmn
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Operator.
Date
Load Range.
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Static Pressure Duct _
Fuel
Tint*
Sample
Point
Load
MW
Stum
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DRY UNCORRECTEO
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Operator.
Date
Load Range-
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Barometric Pressure _
Static Pressure Duct _
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Tim*
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MW
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Date
Load Range
Ambient Temperature.
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Static Pressure Duct _
Fuel
Tim*
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Poml
LMd
MW
Slum
Flow
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1000
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CO
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-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant
Location.
Operator.
Date
Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
Time
SimpM
Point
Load
MW
Slum
Flow
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NO
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NO.
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Barometric Pressure _
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Fuel
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Load Range.
Tim*
SunpM
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MW
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Plant
Location.
Operator.
Date
Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
TlIM
SampM
Point
Load
MW
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Date.
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Fuel
Time
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Point
Load
WN
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Operator.
Date
Load Range-
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct_
Fuel
Tim*
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Load
MW
Slum
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Aerotherm
Plant
Location.
Operator.
Date '.
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COMMENTS
<"'.vJ/.ir-( t'-K'f"1
AVERAGE
f
01
0.1.-' I /8J
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant
Location
r./n .
pate ?--"-
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel !*. ts. c i
Load Range.
Tim.
SwnpM
Poml
LOMl
MW
Staim
Flow
Ib/ht
alOOO
DRV UNCOARECTED
CO
ppm
80,
NO
ppm
NO.
ppm
NO,
ppmn
CORRECTED TO
V, O2 DRY
NO
ppm
NO.
ppm
NO,
ppm
HYDROCARBONS (HC)
Tolll
HC
MallMiM
Non-
HC
T
Suck
Qu
T«mp
f
COMMENTS
/M.M
(', S >-/
It-ff,
z.c-
V"
01
ro
(3 6-.
O2d
fee.-)
nzi
t-
V
c /
-------
FIELD DATA SHEET
Aerotherm
c- -
1
1
1
4>
Ul
CO 1
>lant r lv f . i c-^.v. (^ £t IC\
.ocation
Operator
Data ~
Load Ra
Tim*
Z<3k
zlfl
~LZ.c.£>
Z.rxi/
2Z.SC-
?T2*r<
3V&.
2?>Z.\
Z2>36>
7-$T/
^j^ C,^
f^.fKn*-*^
L - r / - 6^
ngA
Ponl
Lotd
MW
SlMm
Ftow
Ib/lu
»IOOO
Amt
Bare
Stat
Fue
OKI UNCORRECTED
»
Z Z-
2;t/
^ «v
Z.-'T
"Z-%
Z..^
7 -(
z.b
?,~5"
'? *S
%
^^ t-
/'T.o
/^l O
jy.^-.
m fa
I^.'S
\ t-J ^/
/y (^
l<-/,d/
i?..;i
CO
PPm
II. ''6
&.c{
\7,f.
\-JfJ
tc>. c
i3 /
j \^Cf
i '^f'l
2,1,0
7V
r*
~?LI~7
~73^
7^2,
"7Z"^>
-7/s"
7*f Z.
~>H
"/"i
71=.
NO
ppm
ppm
777
72.5
77.^5
7*V/.
ppmn
CORRECTED TO
y, 02 DRV
NO
PPm
NO,
ppm
N02
ppm
>ient Temper
>metric Press
ic Pressure (
/ cr e-
HYDROCARBONS (HC)
Told
HC
Meihana
Non-
MaUiarw
HC
S
Slack
Qu
T«mp
F
L/jj;)
'-wr
<~ifyi->
(./^L/
"i
-------
f
01
FIEL
\
Plant C-.Kt-Ljrni'V ( tiv\f\
Location
Operatoi
Date
Load Ra
Time
&or>6>
OOL-I
(DO'^
COS/
t>
013.1
r>/sV
r,-2L("d>
tv^?(
^25^,..
Oe-S~l
O'3o£-
rf*>t|
Su S r"A«t
I ' r /*"\ i L f*>u c- (v
£ I
t - g*-y
Sample
Point
Load
MW
Sleam
Flow
Ib/lu
xlOOO
1
D DATA SHEET
Ambient Temper
Barometric Press
Static Pressure C
Fuel /-t^
DRY UNCORRECTED
5
/.*7
~L.~~)
"?.,6
Z..O
Z..?4
2,.6
"Z,(
v .^
7- .-7
Z.V
"Z.1-/
2.."!
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-*_
d, ^
co2
/^-'S'
ivr
l?>.z.
(3/3
/^3
I3.-T
<2.->
i^ o
l?X
l3.i^
tZv"~7
(2-S<
It.U-
S"T"
CO
ppm
34 .C
/-J,^
10^
V>"
|^><-/
/^.6
^^ >, j
(^,<-/
T(V
Z2.Z
'^"Z
?_.q,y
5^-7
V /
so2
ppm
7K-
~?ll>
~?/^
"7?2
~7d
76*>
~7^>V~
"71 "2
fill
fe72
tfo?
£>/'
(&V-i
*> c.
NO
ppm
1
ppm
-/Xu^
ppcnn
COI
NO
ppm
IRECTED TO
. O2 DRY
NO.
ppm
ppm
£\ ACUREX
''r* Aerotherm
atura
ure
)uct
HYDROCARBONS (HC)
Total
HC
-
Methane
Non-
Methane
HC
Y
Slack
Oa>
Temp
F
VS1^
1^2
Li(i'*)
t-CZ^l
t~l%^
>-/'3l 1
t &t{
COMMENTS
/osf M -/^ fiyS-X^fe
/v> j_ il fa* 18 1")
Srt-. ^flp«v> ,i"«»v\
t<-/ .SV> w-f
<-'/i :. <-v -.-A -f-hv; f.-. f-,v
-------
f
I
«
*>!
tTi
1X1
FIELI
>lant l._k«?ii >i-ifv. fg^ec^
.ocation
Dperator
Date
Load Ra
Time
/-7O«.
»?/&'
/7^"5>
"?'/&
f*.L>'*>
K { *
l%1&
/#^§T
/q^/<,
fylK
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/fjLffc
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2£*fc-
70*5
£6x/2S
7Lf£>'*>
71 «
zy^fc
ZZ.05
"> 2 I**
2.7. 3.^
r..2.t/£^
ZSo'i
sws ^
r , ;T\ , L fS u r i^.
«^-/5y^K - .^
ngn
Sample
Poinl
Load
MW
Steam
Flow
Ib/hr
.1000
3 DATA SHEE
Amt
Bart
Stat
Fue
DRY UNCORRECTED
%2
33
7.V
^ °r
P..Q
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^. 1
'?,C>
^ z_
^."2.
33
-^ -?
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^ 7_
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3 '-b
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/u, ty
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/H'3
CO
ppm
so2
ppm
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S~?T
^t-/IC1
AC > "-/
C5 "V
C.'.C
T-/ ^
6 :!./
^57?.
/* > t/
< W 9
f,a,-s<
N02
ppmn
CORRECTED TO
3". O2 DRY
NO
ppm
,
ppm
ppm
r
>ient Temper
>metric Press
ic Pressure [
C± ACUREX
"T > Aerotherm
fiturft
lire
tlIRt
HYDROCARBONS (HC)
Total
HC
Molhane
Non-
Methane
HC
S
Stack
Gas
Temp
F
i-l <.(£,'
tc't'7
<-(<-{({,
<~i ^9
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J_/ X 4"*^
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^^ 4_-U '
v/v.
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t-'<.f:/
COMMENTS
fAr-,-,,^^1, ,(- r.^.^r-
R,,rf <-,,-\ r^-V r*ST«
2. - (V - &'/
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F>-t "Si.K. c-t^- \< \
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C.V< d'MiS'.f-i
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A
AVERAGE
A
032 1/82
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant
(Tk-
Location_SLU
Operator_£_L.
Date
C'l
rMiihL
z. -/s~-
Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
-P>
01
C7>
TIIM
^tf
2^*St
?..^V&
1
^^^rtia^
Sampto
Point
LOW!
MW
SMam
Flow
Ib/hr
1000
DRV UNCORRECTED
°a
%
'.?H
3-O
3'z-
co,
«
n^
/Y.7
K'V
CO
ppm
802
ppm
V5^
G$r
S^V
NO
ppm
NO,
ppm
to*
VV,1
a?
NO,
ppmn
CORRECTED TO
3*. O2 DRV
NO
ppm
NO,
ppm
NO,
ppm
HYDROCARBONS |HC)
Toltl
HC
Meltuiw
Non-
Mallune
HC
H20
S
Suck
a«
T»mp
f
V£*>
COMMENTS
AVERAGE
032 |/82
-------
1
1
I
1
01
FIELI
IT"L f N
'lant ai K " rvv-^ ' ^ *» r* i
.ocation
Operator
n»»A
Load Ra
Tim*
y^d\>
Oo/V
£>/->"% "^
flOc/?r
fVC<>
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tvo}
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6"T/ V
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£.»(<: '>
C^«=? . /
"? ^>
-^,i~i
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3, <..)
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3.i
3, \
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1 ,>
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> i
%
IQ (>
I'-t'-i
t^.^
t<-i.L
I«W^
J Jj ?
i ^tlJ 2
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m.o
m.o
/-/. /
/c./2_
/ty 7
1 ^J ^t
/*y.i
/*-r !X
/L1-'3
h ^
/v
/(/, 2
/CK /
("V?
/ "5i V
CO
ppm
SO,
ppm
^'W
T/*/
CJk^
k/T,
sx/^
S7?
Tfc i"
*>"-O
^vC,
S"S"V
VCc
'i6C
T(iC
-76 '/
-'^3
"^^
<>2M
S ^/
NO
ppm
NO.
ppm
';H T
Sx/ '^
^ '/ ^'
rV ", "?
b"K ?
LO?
crt] >
iOcI
("i <
('-^ ?
C ^ '/
(-0. 7
r ^ »'
£.'J dy
/; ? c
t-^1^
i-Vf
6^.^
L6-i"
£9^,
^.^ t/
-7/.-6
~>\,L
.
NOZ
ppmn
CORRECTED TO
3*. O2 DRV
NO
ppm
NO,
ppm
NOj
ppm
r
>ient Temper
>metric Press
ic Pressure [
r\ ACUREX
*O Aerotherm
aliirn
lire
lnr»
HYDROCARBONS |HC|
Total
HC
MelluiM
Non-
Melhan*
HC
S
Stack
QM
T«mp
F
C-((.\
C/W
HCI
<1(^
<-i~K
LfC^S
if?/
<-^C7
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^ it i
COMMENTS
OA! cl.^S
0-2_-~7.2o'%-
( <-, _j_ = i K c«v Vv-
c.,. . - -,-c/ ^ AV.-X
(\/r i - ^/('i / p/\-A
^£J>-- r fT~ S (o. p r' 1 u-U- < /"
srpA^ri^jt-fc'
o^r-
~?«.fcs 50/YlO
C>2_ "^ ^ '^'^
Co?
5^i 2_
Clcjr .3fp/n "S^PAn.
AVtMAf.E
-------
FIELD DATA SHEET
Aerotherm
Plant
U IOif>/*S«~v.
f
> 4
Location.
Operator.
C.r\
LL
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct_
Fuel
Load Range.
TlIM
C6/8
0A
Vjr'ii
O7-J3
ft-7^X
'.^"-''j.
( *>i a
SwnpM
Pomt
Laid
MW
Si««m
Flow
Ib/lw
mooo
DRV UNCORRECTEO
*
"5.2.
3,2.
7
|3>>
/3-7
f*.*
i^i»
|3. 7
/?,»
B.9
Tr^^
CO
ppm
f.Uf
80,
ppm
wr
^yi
r/cf
S3V
i^
^"^^
'iJV
^S"
r-
NO
ppm
NO,
ppm
fit*)
72.C.'
7-tf
St-.B
^3 7
5"V,f
y(.-r
S5.<^
NO,
ppmo
CORRECTED TO
3". 02 DRV
NO
ppm
NO.
ppm
NO,
ppm
HYDROCARBONS (HC|
Total
HC
Mclluna
Nan-
HC
H,0
Suck
Qu
T«mp
F
W)-i
^V?
^^
-t^o
COMMENTS
AVERAGE
032 |/62
-------
FIELD DATA SHEET
Aerotherm
Plant
Location
Date
? "ML"
Load Ranc
Ambient Temperature
Barometric Pressure _
Static Pressure Duct _
Fuel
Tim*
Sampo
Point
MW
Stum
Flow
Ib/hr
1000
DRV UNCORRECTEO
CO
ppm
80,
ppn
NO
*».
ppm
ppmn
CORRECTED TO
3*. O2 DRY
NO
NO.
ppm
N0a
ppm
HVOROCARBONS (HC|
Tout
HC
Maihana
Non-
Mclham
HC
SUCk
Oat
T»«ip
F
COMMENTS
Z-7
"72^
/&-/ i- .-
l&.t
S< -
'50
6V"?
"V k c 1 .-\
f ..( Ji((\
657
d bf>iA-
CO? - i
6SV
"i.S"
G~lO
AVERAGE
032 1/82
-------
FIELD Di
Plant C_l\ oi.Jr^CS'-V- (rdR. 1
f
O.
Location
Operato
Load Ra
Tim*
'^!2.Q
1 4«y v
J^f^Cj
/'?/*/
;~?a«y
/Wv
/7S*?
/ %/ v
/^VT
/6W
(ft&C/
/'9/">/
1*1 T.S
/q-*y
fdf^c.
^Pl<~/
tx #10
£ ^
3,/'Y
3»y2-«?
C^/^r/jy
"Z./ i"9
~2-Z.L>4
3,3,^
S" US - 6:CC
r C"l . r"\l/
3.7
^.S"
3.7
Cl v6
Xa"
.7,-T
coa
B. v
/3.-V
137
;1 C
I5- '
/ ^.v
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i*> 2.
|5.3
/ i.3
1 ^. £,
/ ^ /;,
,% \ .-
i^^i
/ 3>. ^
I '?> x
1 V2.
i "?.r-
/"X.-i-
1^7
i:\.L
IJL.6
I"X 1
co
ppm
\
^'/""l-
802
ppm
ft*-/
(.-II
:*i
C* » C^
At / >
/ o* vTl
C-f-t.i*
((: -^
O.-7
7 !.<-(
NO,
ppmn
\TA SHEE
Amt
Bare
Stat
Fuel
CORRECTED TO
3", O2 DRY
NO
PPm
NO,
ppm
NOZ
ppm
r
)ient Temper
>metric Press
Ic Pressure C
^ ACUREX
^T* Aerotherm
alura
urn
liiftl
HYDROCARBONS (HC|
Tol«l
HC
Molhino
.
Non-
Mclhifw
HC
^
-fe-
^
&
&
-b~
<^-
_£y
^»-
'^-
T
Stack
ou
Temp
F
COMMENTS
AVERAGE
032 t/62
-------
FIELD DATA SHEET
ACUREX
Aerotherm
Plant
T». l(-lO I*V
S,/s Ci
npnrqtnr C"... t^Nu O.t.-.V
"X -
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
Load Range.
Tim*
2ZW
a.^^v
a^yw
Dtfz<*
.^ty^
^3^
Sunpto
Poml
Lead
MW
Slum
Flow
Ib/lu
1000
DRY UNCORRECTEO
°2
%
1 *
"7 1
D.-r
1.7
1.7
^>
CO
ppm
so2
ppm
K?/
f V9
r^f
( (7
^r
n,-r
NO
ppm
NO.
ppm
'TT'O
7 < i
'??<-
7> ?
7Vt>
7
G>-
&-
-e-
&r-
HZO
V
Sue*
Qu
Temp
F
COMMENTS
AVERAGE
(XU
-------
FIELD DATA SHEET
Aerotherm
Plant
Location.
Ambient Temperature
Barometric Pressure _
Static Pressure Duct.
Fuel I
Load Rangeu
TlIM
Swnp*
Ponl
Load
MW
SMMI
Flow
Ib/hr
xlOOO
DRV UNCORRECTED
CO,
CO
ppm
SO
NO
ppm
ppm
NO,
ppmn
CORRECTED TO
3*. 02 ORV
NO
ppm
NO.
ppm
NO,
ppm
HYDROCARBONS (HC)
Tout
HC
Mairurw
Noo-
UdhaiM
HC
Suck
On
T«np
F
COMMENTS
OCX*-/
(OM
3
\.a
ib
ea
A'ff.f.*
v r?
lor
71 ?<
Ol
-X
a -7
fcV 5
±LU-
a '
o-
3-9
Q 2-.
.
Cf,/*/
S*
AVERAGE
032
-------
FIELD DATA SHEET
Aerotherm
Plant
Location.
Operator.
-? -
Load Range.
Ambient Temperature.
Barometric Pressure _
Static Pressure Duct _
Fuel
Tim*
Simpl*
Poml
L(Md
MW
Slum
Flow
Ib/lu
«IOOO
DRY UNCORRECTEO
CO
CO
ppm
so2
ppm
NO
ppm
NO,
ppm
N02
ppmn
CORRECTED TO
3'. O2 DRY
NO
PPm
NO.
ppm
NO,
ppm
HYDROCARBONS (HC)
ToUl
HC
Non-
Melhano
HC
H20
StKk
On
Temp
F
COMMENTS
fif, .7 -/
3.6
&.<&*
t- c>
iis.tr
O1:
U
6 OS
a. 7
O.S
a -9
UL
<=OL
i-r
B3J.
£23.
2. «TO
7,2'
AVERAGE
032
-------
FIELD DATA SHEET
£\ACUREX
T* Aerotherm
Plant
Location
Operator.
Date
Load Range-
-o.
Ambient Temperature ££.
*""i <3f
Barometric Pressure -*, I-
Static Pressure Duct
TlIM
SunpM
Potnl
Load
MW
Sl««m
Flow
Ib/lM
« 1000
OHV UNCOflRECTEO
CO,
CO
ppm
802
ppm
NO
ppm
MO,
ppmn
CORRECTED TO
3*. O2 DRY
HYDROCARBONS (HC)
NO
ppm
NO
NO,
ppm
TOUI
HC
Non-
MattMiw
HC
Slack
Q«
T«mp
f
COMMENTS
Ai*«
701
123
klL
illZ
Ot
7rl
vn
/a.-?
3 .-7
If-
a. 7
a -7
FeS
AVERAGE
032 1/82
-------
4.2 FIELD DATA SHEETS FOR EPA METHOD 5/8, SASS, YOST, ANDERSEN IMPACTOR,
CONTROLLED CONDENSATION (CCS), AND EPA METHOD 7
4-65
-------
FIELD DATA
Page / of
Plant_
Date
Sample Location
Sample Type
Run Number
Operator
Implnger Volumes
Initial Final
Net-Gain
Probe Length and Type
Nozzle Size & I.D.
Pltot Coefficient I I.D.
Assumed Moisture //
Ambient Temperature_
Barometric Pressure_
Static Pressure, (H?0)
Filter Number(s)
Hg, tCy $
Final at 75"""" Hg. >0fl7
Pltot Leak Check: P.JVT
SASS Condensate
Total Volume
MNdV
- "<"d>4 ({f)
( P)
Clock Tine
(24-hr)
Clock
Temperature °F
Orifice Pressure
Differential
. In. Hrt
Gas Meter
Reading
(V.). ft 3
Velocity
Head
Traverse
Point
Number
PlMO
Vacuun
In. Ho
-------
Page A- of
Clock Time
(24-hr)
Clock
Gas Meter
Reading
(V.). « 3
Init.
. ,25-
Velocity
Head
(AP«).
in. JfeO
Orifice Pressure
Differential
(AH). In. H20
Desired
A 7 a.
Actual
A 7
Temperature °F
Stack
Probe
Inplnger
S
Organic
Nodule
Oven
Gas Meter
In
Out
Pump
Vacuum
In. Hg
Avg.
en
.5*6
-2.5
.0
*?
/> / g.
//
5V
070
765,?
775.
A
A2>
Dun No.
/
Contents:
777-.
Sampling Location
-------
FIELD DATA
ft 3/6
Page ^_ of
Plant
Date
Sample Location
Sample Type
Run Number_
Operator
Implnqer Volumes
Initial Final
5&0.0
Net Gain
Probe Length and Type__
Nozzle Size & I.D. »3O9r
Mtfc,
/LLz
-------
Page ,J2- of J2-
Traverse
Point
Number
Clock Time
(24-hr)
Clock
Sampling
Time, min
Gas Meter
Reading ,
Inlt.
Velocity
Head
(APS).
in. H20
Orifice Pressure
Differential
(AH), in. HjO
Desired
Actual
Temperature °F
Stack
Probe
Impinger
Organic
Module
Oven
Gas Meter
In
Out
Pump
Vacuum
in. Hg
Avg.
3
n.
22
ff
/x
2-5?
il
,2 1
s/
10
ss
?3
JLu.
,353
2.
Z
3L
53
3-05
.30
73.
^
7
Run No.
Consents:
Date
'4/f
Sampling Location
-------
FIELD DATA
Page
o
I of
Plant
Date
Implnger Volumes
Initial Final
Net Gain
Sample Location
Sample Type
Run Number \
Operator
Probe Length and Type \S £/ >
Nozzle Size & I.D. C
Pltot Coefficient .& I.D.Q.gl4
Assumed Moisture If '4P
.471
Jl
n
/.I
I-S
.432-
,^O
'cf
17 ,<£>.
Hoo.b
er/
375
/« ,(53-
A tjars5.\vX«^\_ ^«Ov*». O«^
Comments: »»:«
m^^( -iJjtx^ COfxXxM.^?e,
7602/5/e Sev 1
-------
Page 3 Of
Traverse
Point
Number
Clock Time
(24-hr)
Clock
Sampling
Time, mln
Gas Meter
Reading
Velocity
Head
(APS),
In. H20
Orifice Pressure
Differential
(AH), in. HaO
Desired
Actual
Temperature °F
Stack
Probe
Implnger
Organic
Module
Oven
Gas Meter
In
Out
Pump
Vacuum
in. Hg
Avg.
v£P~
Ao
l-l
STL
5-K
C'<
5^0.7 >-
15
Hfo
.HO
4/0
166
30
-HO
$7
CQ
53
.HO
n
Run No.
Conments:
Date
IH<5C>
Sampling Location
-------
Volatile Organic Sampling Sampling Train (VOST) Data Sheet
Plant
Date
Cfn£0
Project No. 30 77&S'.S'S
Operator /77. ff.
Sample Location
Run No.
Una
fac.kart,
Darowtrlc Pressure (In. Hg)
Ambient Temperature (*F) (0 0
Trap
Set
Trap
l.D.
Clock Tine
24 Hour
Elapsed
Time
(minutes)
Dry Gas
Meter (L)
Volume
Sailed (L)
Temperature (°F)
OGH
Probe
Heated
Line
Tenax
Inlet
Rotoneter
Setting
Pump
Vacuum
(In. Hg)
Leak Rate
LPN at Vacuum
Contents
Start:
i ft
610
to
£»
ro
a 00
31 <*
*>*
stirt!
Stop: _
fA
*
**
u
stop!
M
A//)
4
TA
QionL.
*>*
Alfl
#0
o.f
>/t 2-nd
Start:
stop:
Summary
X
aft*
- not .
-------
Volatile Organic Sailing Sampling Train (VOST) Data Sheet
Plant.
Date
ifi/ff
Project No.
Operator
Sanple Location,
Run No.
(U&A
Barometric Pressure (in. Hg)
Ambient Temperature (BF)
Trap
Set
Trap
I.D:
Clock Tine
24 Hour
Elapsed
Tine
(minutes)
Dry Gas
Meter (L)
Volume
Sampled (L)
Temperature (°F)
DGH
Probe
Heated
Line
Tenax
Inlet
Rotometer
Setting
Pump
Vacuum
(in. Hg)
Leak Rate
LPH at Vacuum
Comments
*""
/*;/
n
U/fi
Al
/
~7i]A
CO
if'
76
"I*
y»_
Start:
Stop:
Start:"
Stop:
sTartT
Stop:
Summary
Notes:
-------
Corporation
ANDERSEN FIELD TEST DATA
Plant
Test Location.
Run No
Date.
Operator.
Molecular Weight
% H20 _
Nozzle Size & No.
Pitot Coefficient t
Pilot No..
Ambient Temperature
Barometric Pressure.
Static Pressure (Ps) _
Filter Set No. :
Meter Box No..
Orifice Coefficient.
,6*7
"Hfl
/.
SAMPLE
POINT
NUMBER
CLOCK
TIME
SAMPIE
TIME
VELOCITY
HEAT
AP in. wg.
ORIFICE
METER
AH in. wg.
GAS
' METER
VOLUME FP
TEMPERATURES °F
STACK
PROBE
IMPINGER
GAS METER
IN
OUT
PUMP
VACUUM
In.Hg
COMMENTS
6
£7
6
^*\ s
-------
Corporation
Plant _
Test Location _
Run No P*->
Date.
-^ 7
Molecular Weight
% H20
Operator
Nozzle Size & No.
Pitot Coefficient
Pilot No.__
Meter Box No.
ANDERSEN FIELD TEST DATA
Ambient Temperature
Barometric Pressure
Static Pressure (Ps)
Filter Set No.
Orifice Coefficient__t^ZL
SAMPLE
POINT
NUMBER
CLOCK
TIME
TIME
VELOCITY
HEAT
^P in. wg.
ORIFICE
METER
4H in. wg.
GAS
' METER
VOLUME FTJ
TEMPERATURES °F
STACK
PROBE
IMPINGER
GAS METER
IN
OUT
PUMP
VACUUM
In. Hg .
COMMENTS
o.
&e4a*j£^'-ijxif
£4.
sj
tn
ASA
30,0
97S.SS/
y
forni FPO-r»7n H fi 79
-------
CONTROLLED CONDENSATION SYSTEM (CCS)
FIELD DATA SHEET
Plant
Date
Sample Location
Run No. l_
Operator
Ambient Temperature
Barometric Pressure ^2ft
Meter Box Number
Meter Orifice Coefficient
Meter o Factor /
'«*/»'%/
C**W<0
Clock Time
(24-hr)
clock
Sam-
pling
Time,
min
510
Average
Gas
Meter
Reading
Init.
97*. 719
Temperature (°F)
Stick
537
Probe
£75
5^5
Filter
ftt
a?
ut
Jod
Recirc
Water
ilU-m
i*
IfO
m
Sl't /SO
Exit
Coil
t
Dry Gas
Meter
In
GJ
Out
e.f- £
**-*
*.<*-£>
O.'t- £.S
5>,f 7
** 7
0.9-7
7
Sf
C6.fr? ₯
902292
902296
4-76
902291 ;
902295
-------
CONTROLLED CONDENSATION SYSTEM (CCS)
FIELD DATA SHEET
Sample Location Tl/S-C>7 A.
Run No. SL
Operator
Ambient Temperature
Barometric Pressure
Meter Box Number
Meter Orifice Coefficient^
Meter a Factor /O6Q
902301
- ~
902302
~77.902293
902298
-------
ACUREX CORPORATION
Run Numb«f
Dote /"
NOX SAMPLING
PROBE
Unit No. Length =
Lining
Material
Pre-Filter
Heated
Pitot
Tube
ft D S. Steel 0 Glass Wool 0 Yes No. */4
D No
Flask No.
Volume of Flask
Less Absorb. Soln.
initial Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
D
SAMPLING DATA
SL
Coefficient:
D -85 D
"7O
-70
-7^2-
. Z.
.0.1
OA:
ox:
~PtffeL,*)M
por-t
mmm
4-78
-------
D Kl , NOX SAMPLE RECOVERY
Run Number j *ANQ ANALYS,S
SAMPLE RECOVERY
Flask No. 3. 2S"
1?
Final Conditions:
Barometric Pressure (in. Hg) _^-J-5~O J9.rO S-tySTO
Flask Temperature (°F) 6^f ~7f TJ_
Flask Vacuum (in. Hg): -
Top 0. 2 a.?. o,$"
Bottom C.? O.I
o. 1
Difference I-O O^ n"Z"
Sample Number 9<3I3hohrme.lYi-ij-S«4
Analyzed by A^rv^rw fy->rv\n^
Comments:
^^ 7
3-l-ST-SV
mr^nv
4-79
-------
ACUREX CORPORATION
Run Number
Dote /-
2,
NOX SAMPLING
PROBE
Unit No. Length =
Lining
Material
Pre-Filter
3
ft D S. Steel 0 Glass Wool
Pyex pi
SAMPLING DATA
Flask No.
Volume of Flask
Less Absorb. Soln.
Initial Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
^9.65"
#.$(,,3
-70
QK-
OK:
/-*"
Heated
Pitot
Tube
Yes No.
No Coefficient
D .85
13.
/.*"
4-80
-------
3 s-.
Run Number
NOX SAMPLE RECOVERY
AND ANALYSIS
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flosk Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as NC>2 (ug)
Analysis Date
Analyzed by
Comments:
SAMPLE RECOVERY
1
r
O.i.
a. 2.
0.3
a***
ANALYSIS
O
0.3
O./
90; ^03
QC/WO3
4-81
-------
ACUREX CORPORATION
Run Number 3
Date
NOX SAMPLING
PROBE
Unit No. Length =
3
Lining
Material
ft D S. Steel
0 Pyrex
Pre-Filter
Heated
Pitot
Tube
Glass Wool 0 Yes No. fJ/A
D No
Flask No.
Volume of Flask
Less Absorb. Soln.
Initial Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
SAMPLING DATA
ft??
TO
-?r
IS.S
13.1
0)1
OK.
I.*"
/3<3/ .
A5
4-82
Coefficient: /
a .ss n »/A
/3
£0 7
-79
X-s
-------
Run Number
NOX SAMPLf RECOVERY
AND ANALYSIS
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flosk Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as NC>2 (ug)
Analysis Date
Analyzed by
Comments:
SAMPLE RECOVERY
62.
13
C.(e
0 -fc
o.z-
/in
ANALYSIS
o
a-tx-84 3-is-s^
oss
ohiU"inQ
4-83
O.7.
0,3
of
-------
ACUREX CORPORATION
Run Number
Dote
-------
Run Number </
NOX SAMPLE RECOVERY
AND ANALYSIS
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as NO2 (jig)
Analysis Date
Analyzed by
Comments:
Joss
SAMPLE RECOVERY
-JO
-72.
1.2
o.t,
ANALYSIS
. C
mmcn
o.y
0.13?
3-/S--.JV
f
4-85
-------
ACUREX CORPORATION
Run Number
Date
;-jLq-,f<
NOX SAMPLING
PROBE
Unit No. Length =
Lining
Material
Pre-Filter
Heated
Pitot
Tube
ft D S. Steel S Glass Wool S Yes No. O//9
(3 Pyrex rI D No Coefficient:
D -85 0 /i^t
SAMPLING DATA
Flask No.
Volume of Flask
Less Absorb. Soln.
Initial Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
IO
30
Ti-
72-
13.1
13-0
olc
4-86
-------
Run Number
NOX SAMPLE RECOVERY
AND ANALYSIS
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as NC>2 (ug)
Analysis Date
Analyzed by
Comments:
SAMPLE RECOVERY
to
~73
0.9
a.i
a.?
/.r
ANALYSIS
\ C
0
Ko4.l
30
1.0
. fe?
s-
4-87
-------
3c
ACUREX CORPORATION
Run Number
Dote I
NOX SAMPLING
PROBE
Unit No. Length =
-A
Lining
Material
ft D S. Steel
[x] Pyrex
Pre-Filter
Heated
Pitot
Tube
Glass Wool
Yes No. /J//1
No Coefficient:
n .85 a
Flask No.
Volume of Flask
Less Absorb. Soln.
Initial Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
SAMPLING DATA
n
2-oSl
,. 2,
. 2-
Csn /?
-------
Run Number 4,
NOX SAMPLE RECOVERY
AND ANALYSIS
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as N©2 (us)
Analysis Date
Analyzed by
Comments:
SAMPLE RECOVERY
n
a/
a. 3
O.I
o./
0-3
/-^r-yv
/3/a
/V30
ANALYSIS
f
O.IMI
G
0
4-89
-------
ACUREX CORPORATION
Run Number
Dote \~
~7
NOX SAMPLING
PROBE
Unit No. Length =
3
*>/*
Lining
Material
ft D S. Steel
0 Pyrex
Pre-Filter
Heated
Pitot
Tube
Glass Wool
SAMPLING DATA
Flask No.
Volume of Flask
Less Absorb. Soln.
Initial Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
(js. (s>
IZ.9
(3.0
ok_
Cfr>
not
,ni6
4-90
Yes No.
Coefficient:
D .ss r
ILs.2.
,[731
-------
307735.
Run Number *7
NOX SAMPLE RECOVERY
AND ANALYSIS
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as NC>2 (jig)
Analysis Date
Analyzed by
Comments:
F/asb
SAMPLE RECOVERY
If
-70
0-0
0.3
0
O.fc
t-j.
nomm
ANALYSIS
ph c^ZO K,cfT t C
£>.|3I
O
4-91
-------
307-735-^)
ACUREX CORPORATION
Run Number
Date i-
NOX SAMPLING
PROBE
Unit No. Length =
Lining
Materiel
ft D S. Steel
0"!
Pre-Filter
Heated
Pitot
Tube
Glass Wool L^ Yes No. £_
D No Coefficient
.85
SAMPLING DATA
Flask No.
Volume of Flask
Less Absorb. Soln.
Initial Conditions:
Barometric Pressure (in.
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
Hg)
(a?
/3.O
0/C
Crv,
cinamc
4-92
-------
3o~?
Run Number
NOX SAMPLE RECOVERY
AND ANALYSIS
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
SAMPLE RECOVERY
ao
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as NC>2
Analysis Date
Analyzed by
Comments:
03
0,3
ANALYSIS
t c
O.C1?
o
/V^W^ rv\
-71
0.3
0.2-
/33O
4-93
-------
36713*. Fl
ACUREX CORPORATION
Run Number
Date (-"
NOX SAMPLING
PROBE
Unit No. Length =
Lining
Material
Pre-Filter
Heated
Pitot
Tube
ft D S. Steel
0 Pyrex rn
Glass Wool Q Yes No. *)/fi
n No Coefficient:
a .ss n
SAMPLING DATA
Flask No.
Volume of Flask
Less Absorb. Soln.
Initial Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Leak Check
Sampling Location:
Port
Point or Distance from
Inside of Port
Clock Time
Performed by
Comments:
2.3
2 031
13,0
13.0
OKL
/.f
rn/wn
4-94
-------
Run Number
NOX SAMPLE RECOVERY
AND ANALYSIS
SAMPLE RECOVERY
Flask No.
Final Conditions:
Barometric Pressure (in. Hg)
Flask Temperature (°F)
Flask Vacuum (in. Hg):
Top
Bottom
Difference
Sample Number
Date
Clock Time
Performed by
Analysis Procedure
Sample Number
Absorbance of Sample
Absorbance of Blank
Calibration Curve No.
Mass of NOX as NO2 fog)
Analysis Date
Analyzed by
Comments:
t 'If. 3
f/,,-2-
&.0
ANALYSIS
9/0/MZ.2.
4-95
-------
PLANT C
LOCATION
DATE "2
TIME
AMBIENT PRESSURE (IN. H6.)
AMBIENT TEMPERATURE (°F)
SAMPLING POINT '^ ''
TEST NUMBER
OPERATOR
//I,/ 7 /- '/v->?
N0 SAMPLING DATA
Time
/;^j'
'f!O
/rJ*
Flask
Number
t /»
x
«<.*
*~f
/ -
Flask
Volume
(ml.)
?c*o£
IcS"^
2<:Vi.
Initial Conditions
Flask
Vacuum
(in. Hg.)
t'1,.0
-> p -t
'-'- t /
7^rO
Flask
Temp
(°F)
c^ <^~
^ -*
6*5
^o
Final Conditions
Flask
Vacuum
(in. Hg.)
a . cf
/,*>
A
-------
PLANT
LOCATION 5 69
DATE
TIME
AMBIENT PRESSURE (IN. HG.)
AMBIENT TEMPERATURE (°F)
SAMPLING POINT ^ "'.^^r C/Y
OPERATOR
/= //-,'
TEST NUMBER
N0y SAMPLING DATA
A
Time
//rr
A'/i>
/^<
Flask
Number
/*>
f'rJ
! 1
Flask
Volume
(ml.)
7^" ^^
2^'l
-/ -,*~^.
<..* ~^~'
Initial Conditions
Flask
Vacuum
(in. Hg.)
z^fxf
2S-.7
??'
-------
PLANT
LOCATION
DATE
TIME
AMBIENT PRESSURE (IN. HG.)
AMBIENT TEMPERATURE (°F)
SAMPLING POINT 3^ 'v.
TEST NUMBER £*^ ^
OPERATOR
r?
5 7
Ff/vc^-O
2-j^3
:c.?7
Initial Conditions
Flask
Vacuum
(in. Hg.)
2 £ ?
'." "7
'-- 1 I
im
Flask
Temp
(°F)
r/
70
73
Final Conditions
Flask
Vacuum
(in. Hg.)
£W
-/^/a
^ . >
Flask
Temp
(°F)
-^7
60
u>O
4-98
-------
PLANT CXi?>--/-'-vv
LOCATION -5t'rj
DATE ?_~3
TIME
AMBIENT PRESSURE (IN. HG.)
AMBIENT TEMPERATURE (°F)
SAMPLING POINT ',..
OPERATOR
TEST NUMBER
f
NO SAMPLING DATA
Time
r^c^
/ X»J> ^
f*ito
(ViC
Flask
Number
i'
^
rr3
Flask
Volume
(ml.)
/??£
?o^^
7 1^53
Initial Conditions
Flask
Vacuum
(in. Hg.)
??'-*'
^.7
If.t,
Flask
Temp
(°F)
73
^ s
7'^
Final Conditions
Flask
Vacuum
(in. Hg.)
2, /
1,5
0,O
Flask
Temp
(°F)
6f
6±
Cf
4-99
-------
PLANT
LOCATION
DATE
TIME
AMBIENT PRESSURE (IN. HG.)
AMBIENT TEMPERATURE (°F)
SAMPLING POINT -?;,--.
TEST NUMBER
OPERATOR
C.n
SAMPLING DATA
Time
kfO
f&>
I'sSc-
Flask
Number
^3
_u <
j. /
Flask
Volume
(ml.)
- ^ ^ /"
O .- ^ !
Z?-><
Initial Conditions
Flask
Vacuum
(in. Hg.)
r.-r<£
?-~A
?r,<
Flask
Temp
(°F)
70
G!
£1
Final Conditions
Flask
Vacuum
(in. Hg.)
o. a
' /
*~f t~i
(. <"-'
Flask
Temp
(°F)
r- /
X' ->
t ^>
x^ *>'""
^ >
4-100
-------
PLANT C
LOCATION
DATE 2
TIME
AMBIENT PRESSURE (IN. HG.)
AMBIENT TEMPERATURE (°F)
SAMPLING POINT > '-fb
iP^'b
Initial Conditions
Flask
Vacuum
(in. Hg.)
~r,5~
r- s: 5
?f,i
\
Flask
Temp
(°F)
^;c"7
^,p
61
Final Conditions
Flask
Vacuum
(in. Hg.)
/, 7
o, v
A/
Flask
Temp
(°F)
d'c/
^f
^(J
4-101
-------
PLANT
LOCATION
DATE
TIME
AMBIENT PRESSURE (IN. HG.) 2
AMBIENT TEMPERATURE (°F)
SAMPLING POINT
OPERATOR
>.
TEST NUMBER
"7
NO SAMPLING DATA
Time
r A ;,'..'
^-?^
/r*r
Flask
Number
_C
/
7/9
Flask
Volume
(ml.)
/??'/
/996
Initial Conditions
Flask
Vacuum
(in. Hg.)
-zrr
-2r,-6
2 7, "5
Flask
Temp
(°F)
b?
-^ i
/ <7^
1^
Final Conditions
Flask
Vacuum
(in. Hg.)
//^
//6
^3"'
Flask
Temp
(°F)
&>~
££
£-Z
4-102
-------
PLANT G^V/c*-v ( e
LOCATION ?(,<$ £
//-
Flask
Temp
(°F)
<; -,
^.?
C 7
4-103
-------
V-J
PLANT L
LOCATION
DATE
TIME
AMBIENT PRESSURE (IN. HG.)
AMBIENT TEMPERATURE (°F)
SAMPLING POINT lc' ,.-.y\
TEST NUMBER £*'* *1
OPERATOR
/>
N0x SAMPLING DATA
Time
'Z.C/O
L V<- ^
ic^fj
Flask
Number
/>
/6
«7
-
Flask
Volume
(ml.)
.I'o/f
Zo/7
2*77
Initial Conditions
Flask
Vacuum
(in. Hg.)
7 #.Q
2*: i-.
2 ?.£>
Flask
Temp
(°F)
£T
/ ""f
7c/
Final Conditions
Flask
Vacuum
(in. Hg.)
/^ 0
C; c,
Flask
Temp
(°F)
r o
'.' /
^^
£?g
4-104
-------
PLANT
LOCATION
DATE Z
TTMC
(£££;
OPERATOR
r/v (-
AMBIENT PRESSURE (IN. HG. ) '1*1 <
AMBIENT TEMPERATURE (°F) ^
SAMPLING POINT so
TEST NUMBER
NO SAMPLING DATA
A
Time
.^y
12.53
iw'i
Flask
Number
2->
fo
^
Flask
Volume
(ml.)
;e37
2< x,- D
/-/ v-;T
Initial Conditions
Flask
Vacuum
(in. Hg.)
7% -
??^/
~P, ^
/r- /
Flask
Temp
(°F)
£5
61
7^
Final Conditions
Flask
Vacuum
(in. Hg.)
#;*
a- o
?-'?
Flask
Temp
(°F)
y-3
73
73
4-105
-------
PLANT
LOCATION
DATE
TIME
AMBIENT PRESSURE (IN. HG. )
AMBIENT TEMPERATURE (°F)
SAMPLING POINT so
TEST NUMBER x^- i-
OPERATOR
A
NO SAMPLING DATA
Time
,/y-'
/.^/
/S^6
Flask
Number
fO
Cf'2
tt^
Flask
Volume
(ml.)
~^C"0
Z^5 3
i
-------
PLANT
LOCATION 'f'.
DATE
TIME
AMBIENT PRESSURE (IN. HG. )
AMBIENT TEMPERATURE (°F)
SAMPLING POINT ,..
TEST NUMBER
OPERATOR
NO SAMPLING DATA
Time
f <-//</
w
w?
Flask
Number
?A-
-1
it
Flask
Volume
(ml.)
>-, / '
^,
?otef
Initial Conditions
Flask
Vacuum
(in. Hg.)
z.r/?
z«r
Flask
Temp
(°F)
/*>
->^
7,-s
/ w
Final Conditions
Flask
Vacuum
(in. Hg.)
j /
1.1
"V
Flask
Temp
(°F)
c/V
,r
^7
4-107
-------
SECTION 5
ANALYTICAL RESULTS
5.1 Fuel Proximate and Ultimate Analyses
5.2 Particulate and Sulfur Oxides Emissions from Method 5/8 Samples
5.3 Particulate Emissions from SASS Samples
5.4 Particulate Emissions and Size Distributions from Andersen Samples
5.5 Sulfur Oxides Emissions from Controlled Condensation System Samples
5.6 Trace Element Analyses of Fuel and SASS Samples
5.7 Organic Analyses of SASS Samples: Total Chromatographable Organics
(TCO), Gravimetric Organics (GRAY), Gas Chromatography Mass Spectrometry
(GC/MS), and Infrared (IR) Spectra of Total Sample Extracts
5.8 Volatile Organics Analyses of YOST Traps
5.9 NeO Emissions by GC/ECD
5.10 NOX Emissions by EPA Method 7
5-1
-------
5.1 FUEL PROXIMATE AND ULTIMATE ANALYSES
5-2
-------
LABORATORY CERTIFICATE
CURTIS & TOMPKINS, LTD.
ESTABLISHED 1878
Bulk Oil & Chemical Surveyors. Samplers & Weighers
Analytical & Consulting Chemists
SOUTHERN DIVISION
4OI Canal street
'llmington. CA 9O7**-65O3
213-549-674O
29O Division Street
San Francisco, CA 941O3 -4882
415-861-1863
Telex: 171O42
CABLE: ANALYST SFO
FOOD TECHNOLOGISTS
ENVIRONMENTAL ANALYSTS
MEMBERS. OFFICIAL CHEMISTS
AND/OR SAMPLERS FOR GOVERNMENT
AGENCIES AND TRADE ORGANIZATIONS
Laboratory No. 8 4 e3 4
Preliminary No. 7758
Reported 5/3/84
Sampled
Received 3/23/84
For
ACUREX CORPORATION
Report on
1 sample of Fuel
Mark Sample No. 901440
Subcontract No. RB59186A
Release No. 13
Prime Contract 62-02-3176
Acurex Project No. 7951
ULTIMATE ANALYSIS
Carbon
Hydrogen
Oxygen
Sulfur (1st test)
Sulfur (2nd test)
Sulfur (3rd test)
Nitrogen (1st test)
Nitrogen (2nd test)
Nitrogen (3rd test)
PROXIMATE ANALYSIS
Gross Heating Value, BTU per Ib.
Moisture .
Ash
86.2
11.3
0.4
1.00
1.10
1.08
1.04
1.09
1.00
18,430
0.57
0.03
Specific Gravity (API)<§ +60°F
12.6
5-3
-------
5.2 PARTICULATE AND SULFUR OXIDES EMISSIONS FROM METHOD 5/8 SAMPLES
5-4
-------
ISOKINETIC PERFORMANCE WORKSHEET & PARTICULATE CALCULATIONS
Plant CH-6\j/fc,e Performed by
Date £-fa
Sample Location_
Test No./Type /
Barometric Pressure (in. Hg)
Meter volume (std),
\ / y ~+ 460 I
\
(. »i i M.A* /, (& t>*)^T \
[ 5w«&5W\ I\Q*\ ? %\ 4- ' _' \
11 13'6 )
teisW-feU) + 45° /
Volume of liquid collected (grams)
Volume of liquid at standard condition (scf)
Vlc x 0.04707
Stack gas proportion of water vapor
\ std * Vm std < 1 * I '
Molecular weight, stack gas dry
(Tb/lb-mole)
(% C02x 0.44) + (% 02x 0.32) + (% N2+ % CO x 0.28)
C/y,^ x 0.44) + (2,1 x 0.32) + (??.£.+ x 0.28)
Molecular weight, stack gas wet
(Ib/lb-mole)
Mdfl-B } + 18(8 .J. (?fl«r )C\-,et7}'+ 18(/^7^r
Id/0 WO .... ...
Absolute stack pressure (in. Hg)
Pct,rt (in- H.O) (t^/A )
n i 3i.av.iv u i^a »fA +
Pb ' 13.6 » l^4^9 13.6
'b
Vm std
»'c
vw std
wn
Md
Ms
p
^s
,w
5T.^
*,+*»
e»1->*
r^-vc^
1
«.u
6^-Tift
ixi
* * t
7602/5/81/Rev 1
5-5
-------
Temperature stack gas, average (°F)
Stack velocity ffos)
/T.avg + 460
O1^ A 0 IT \ A/4P ^ / - -
00.45 (C ) {/APs ) / p
^ s s
*r , /fetfVZ^ + 460
fl=; an ^,->s \ti TT ^ /.,.. ,., . ._ . . .,
05.49 (OLJd/^T) J^rL,^^
Total sample time (minutes)
Nozzle diameter, actual (inches)
Percent isokinetic (%)
17.33 (Ts + 460) (Vw std + Vm std)
* Vs llfc^s - Nd2 t|.^
17.33 (y/kl+ 460)((^«>^) + (t^7^-)
( ->2. )(v-r.?o )(a^,2^ )( .-s^f"
, -, 3G" fti^As
Area of stack (ft2) *= 3.1416
Trr2 -5- 1 44 , JT ( /fr )2---1 44
Stack gas volume at standard conditions (dscfm)
60 (1 - B )Vs A. / 528 \ / Ps \
wo avg , / T^ avg + 4go i f 29.92)
60 (1 -.tff7l)fcC«Ab^/- 528 \ /^2)\
U5Wf.+ 460/ UZ9.92)/
\ / \ /
Particulate matter concentration, dry (gr/dscf)
15 132 MD(9rams) fl,, ( )
Vm-td ( }
Emissiorr rate of particulate matter (Ib/hr)
0.00857 (QJ C, , 0.00857 ( )( )
- -istd)
Ts
Vs(avg)
0
Nd
%I
AS
QS
r
^c
S(std)
T
- *>
E
H
^5*6,2.
Hr.*2o
"?2.
207
/oT.U
7,0&^
^7^
il
:- iji i '
- - ' \
V
t
7602/5/81/Rev 1
5-6
-------
ISOKINETIC PERFORMANCE WORKSHEET & PARTICULATE CALCULATIONS
Plant c.*£ti/*_#JL^ Performed by
Date a-i-S-4-
Sample Location Qgrt.gr
Test No./Type a ; A?-
Barometric Pressure (in. Hg)
Meter volume (std),
* ' jv)" tC
17 64 ( l( 13.6 1
Volume of liquid collected (grams)
Volume of liquid at standard condition (scf)
Vlc x 0.04707
Stack gas proportion of water vapor
Vw std + Vm std <*s££.J + (Si^lt3
Molecular weight, stack gas dry
(Ib/lb-mole)
(X C02x 0.44) + (X 02x 0.32) + (X N£+ % CO x 0.28)
( x 0.44) + ( x 0.32) + ( + x 0.28)
Molecular weight, stack gas wet
(Ib/lb-mole)
Md(l-Bwo) + 18(BWQ), ( )(1- ) + 18( )
Absolute stack pressure (in. Hg)
Pet^t (in- M) (**-.)
r> x stacA c- I'?f93t+ -»-*-
pb ' 13.6 ' ^-^^ T3.6
Pb
Vm std
Vlc
vw std
wn
Md
Ms
ps
avzv
«..««
,,vr
d»tD ^ (
O. 0*7")^
PA'fc.L'iW /pJA-A
^\ "H* Qs «e 4.
*->.2V
X
,«i
>/«
/«
}
l\
7602/5/81/Rev 1
5-7
-------
Temperature stack gas, average (°F)
Stack velocity (fos)
/T.avg + 460
0=1 AQ (r \ (J~At> \ 1 _. - -
05.40 (Cp) (V4PS } / p
(j S S
^ , /(*"?/) + 460
nc. An ( -?* ) Ij \ / ____,._
05.40 (^L)(^^) J(2m)(£L£|r
Total sample time (minutes)
Nozzle diameter, actual (inches)
Percent isokinetic (%)
17.33 (Ts + 460)(VW std + Vm std)
e vs ps Nd2
W/ *?.J<1
17.33 (^j + 460) ((^u) + (^.gt^)
( 7^ )(V7/?2_ Jf^?^*! )( ,?o9)z
Area of stack (ft2) *= 3.1416
,rr2 -T- 1 44 , ff ( /y )2-^l 44
Stack gas volume at standard conditions (dscfm)
60 (1 - B )Vs A. 1 528 \ / Ps \
wo avg ^ /Tsavg + 460) (29.92)
60 (1 -.of7jr)todfr«f)/ 528 \ / fet«* \
U-)-7./ + 460/ V(29.92)/
\ / \ '
Particulate matter concentration, dry (gr/dscf)
15 439 MD(9ranis) ls 432 ( )
Vm-td ( }
Emissiqn rate of particulate matter (Ib/hr)
0.00857 (QJ C, , 0.00857 ( )( )
' -(std)
Ts
Vs(avg)
B
Nd
XI
AS
QS
r
uc
S(std)
i. .- - - '»
* <1 '
' ED
K
V7%/
v?. sa
72
-3o^
>ot,yy-
7x^^1
*}?<(-
i
r
7602/5/81/Rev 1
b-8
-------
ACUREX
ANALYTICAL REPORT
Sample of:
Sample Date:_JhklH.
Requested By:
I.D. Number:
Analytical Method: 6m\/uner(2-if, Ar>giifse.s a
-------
ACUREX
ANALYTICAL REPORT
Sample of: O.nn ? A / £ fe g.
Sample Pate! 2-1 -
Requested By:
I.D. Number:
Analytical Method:
Date of Analysis: ^lt3 ~
. o4 ttVc -Vhcyj 51 ?
Lab I.D. Number
Component
Analytical Result
Unit
Ail
Q
and
b)AH Ic CO/ r'£ctjz.A
Analysis
5-10 Date
v-
Form EED082 5/81
-------
ACUREX
ANALYTICAL REPORT
Sample of:
Sample
Requested By: Lrtg-gy V*?>ATT cni^5* % I
Analytical Method:
Date of Analysis:
"TTrgflTiads O* &Pft $1$ Xtv»?)O6£q.
g* '6 ' o fr
Lab I.D. Number
TEST * i)
^ oi Ml -L
B\AMIL)
Component
DM rots
,o
Analytical Result
3,^33
C 1 ^>O. »
on
Unit
\QO mcj
1C
1*0.01
N, S O.OlOOfJ
-f Tr
Analysis
5-11
Date.
FormEEO-083
-------
5.3 PARTICIPATE EMISSIONS FROM SASS SAMPLES
5-12
-------
ISOKINETIC PERFORMANCE WORKSHEET & PARTICULATE CALCULATIONS
Plant CHcJ/HJ UfA /=r.;~ i'~-'.-Je.L. Performed by
Date /g-*
Sample Location
Test No./Type
Barometric Pressure (in. Hg)
Meter volume (std),
17.64 /!m\/Pb+^\
\a/\Tm + 460/
l(8a*\ 7&? ) + L£J\
r 61 I ~TIT~
yjL*^)/ \U£_) + 4^o /
Volume of liquid collected (grams)
Volume of liquid at standard condition (scf)
V1C x 0.04707
Stack gas proportion of water vapor
Vw -td W'^
\ std + vm std (2UJ + (Hiz)
Molecular weight, stack gas dry
(Ib/lb-mole)
(% C02x 0.44) + (% 02x 0.32) + (% N2+ % CO x 0.28)
(ft,l x 0.44) + (2-7 x 0.32) + ($k+ x 0.28)
.
Molecular weight, stack gas wet
(Ib/lb-mole)
Md(l-Bwo) + 18(BWQ), (i^iJd-AW) + 18 (£M)
Absolute stack pressure (in. Hg)
r , Pstack «'» H2°' (J?^, . ' >
'b 13.6 ' ( ' 13.6
pb
Vm std
Vic
vw std
R
WO
Md
Ms
ps
7K
/??o
fa*7
$ /3 "3>
3a2_
**?
J??J ^
Form 440 3/84
5-13
-------
Temperature stack gas, average (°F)
Stack velocity (fos) -- ...
/T.avg + 460
R^ Aft (C \ (J~AP \ 1 .-
85.45 (CpJ (V4P$ avgj / p
*J S S
V*. /(Jsrt ) + 460
n^ di id bitwJ } / .....
oo.tj ^,>'u;vv ; / v '
J(?fo )(.»? )
Total sample time (minutes)
Nozzle diameter, actual (inches)
Percent isokinetic (%)
17.33 (Tc + 460)(VU std + Vm std)
o W III
0 Vs Ps Nd2
17.33 (fa + 460)((jty/J + (7^))
( ,"^5 )( ^5,5 )( ^f,S )( Z0.i7/)
Area of stack (ft2) »= 3.1416
jrr 2 -T- 1 44 , * (__ 12-H 44
Stack gas volume at standard conditions (dscfm)
60 (1 - B )V$ A, 7 528 \ / Ps \
wo avg J i T^ ayg + 46Q i i 2g g2 i
60 ( 1 - 6. 13) (£.8 ) (?Pfl )/ 528 \ / & \
H5f, +-460/ V(29.W)7
\^---«* / \ /
Particulate matter concentration, dry (gr/dscf)
15 432 V9rams> 15 432 < >
Vm,td ( )
Emission rate of particulate matter (Tb/hr)
0.00857 (QJ Cf , 0.00857 ( )(
"istdj
TS
Vs(avg)
0
Nd
%l
AS
"s
r
**c
S(std)
ED
p
^-,'6
K.&
2^3
C.iiS
9&s-
7.^9
1&K
5-14
Form440a 3/34
-------
SASS ANALYTICAL DATA
Sample No.
Sampling Location £ei/y*« £; & _ Run No. /
Recovered By feemft^ Recovery Date 2-/-
-------
ACUREX
ANALYTICAL REPORT
Sample of:
Sample Date:
Requested By:
I.O. Number:
Analytical Method: 6f&0tfnfl\f'if-
Of A nalycic- ^/ 9
Sft
. Hers a^d
Lab 1.0. Number
Component
Analytical Result
Unit
a ra..s
o. 0000^
O.
O. GOODS'
Y
Analysis
Form EED082 5/81
-------
5.4 PARTICIPATE EMISSIONS AND SIZE DISTRIBUTIONS FROM ANDERSEN SAMPLES
5-17
-------
ACUREX
cSSn PARTICULATE CALCULATIONS ^J
1. Volume of dry gas sampled at standard conditions, 68° F, 29.92 inch Hg (scf)
Vm
Vmstack -
2. Stack gas moisture condensed at standard conditions (scf)
Vwstd 0.04707 Vl
Vm(B) c* fr I
/7 /
3. Stack gas proportion of water vapor, by volume
B
wo Vwstd*Vmstd
4. Stack gas dry molecular weight (Ib/lb-mole)
/3.-D 3.0
MWd 0.44 (%CO2) + 0.32 (%O2) + 0.28 (%N2 + %CO)
5. Stack gas molecular weight (Ib/lb-mole)
MW8 = MWd (1 - Bwo) + 18 (Bwo)
6. Pressure stack, in. Hg
3G
5-18
-------
7. Stack gas velocity at stack conditions (ft/sec)
= 85.49 (Cp)
46°
8. Stack gas volume at standard conditions (scfm)
Qs - 60 (1 - Bwo, Vsayg As
Ts>av5g2! 460) (gOg
or Qa 60 Vsavg As (acfm) =
9. Test percent isokinetic
%l
10. Paniculate matter concentration, gr/scf
M^
C. = 15.432
S
std
o.cxC?
M
or Ca 15.432-77- (gr/acf) =
vmstack
11. Emission rate of paniculate matter, Ib/hr
ER - 0.00857 (Qs)
&/
12. Percent excess air at sampling point
100 [%O2 - 0.5
% EA =
0.264 %N2 - (%O2 - 0.5 x %CO)
13. Emission rate of paniculate matter, lb/106 Btu
.».**
5-19
-------
ACUREX
Corporation PARTICULATE CALCULATIONS
1. Volume of dry gas sampled at standard conditions, 68° F. 29.92 inch Hg (scf)
AH
Vmstd
2. Stack gas moisture condensed at standard conditions (scf)
Vwstd = 0.04707 Vlc =
3. Stack gas proportion of water vapor, by volume
B.
VwStd
wo - vwstd + Vmstd
4. Stack gas dry molecular weight (Ib/lb-mole)
f?f f J^j?
MWd = 0.44 (%CO2) + 0.32 (%O2) + 0.28 (%N2 + %CO)
c3 G
5. Stack gas molecular weight (Ib/lb-mole)
- Bwo) + 18 (Bwo)
6. Pressure stack, in. Hg
P, =
13.6
5-20
-------
7. Stack gas velocity at stack conditions (ft/sec)
Vs = 85.49 (Cp)
8. Stack gas volume at standard conditions (scfm)
Qs - 60 (1 - Bwo) Vsavg As (T 52*46Q) 4£
\ S,3VQ j \
or Qa 60 Vsavg As (acfm) =
9. Test percent isokinetic
92
10. Particulate matter concentration, gr/scf
M,,
3s = 15'432 Vm
'std
ME
Vmstack
or Ca = 15.432 p (gr/acf) =
11. Emission rate of paniculate matter, Ib/hr
ER = 0.00857 (Q_) C.
12. Percent excess air at sampling point
100 [%O2 - 0.5
% EA =
0.264 %N2 - (%O2 - 0.5 x %CO)
13. Emission rate of particulate matter, lb/106 Btu
E = 2.679 x 10* nT^y - V209^^02
)
5-21
-------
^ACUREX
Corporation
ANDERSEN PARTICLE SIZE ANALYSIS
Plant
Test Location.
Run No /
Flow Rate
Tare Weights:
Final Weights:
,
/,.
By.
nation
STAGE
NO.
FILTER
NO.
FINAL
WT
(g)
TARE
WT
(9)
SAMPLE
WT
(g)a
% OF
TOTAL
WTb
CUMULATIVE
% OF TOTAL
Dp
/, 23
tfCP-
/, 2 1 7CO
/,2f362-
2/
/. 7 /
ii
(5 -
/, 22
Ucp-21%
-7.
«? -CC-935
TOTAL WITH FILTER
TOTAL WITHOUT FILTER
Blank correction value = '
Blank correction value
~ 0.
Stages 0 through 7
Stage F (final filter)
^Includes appropriate blank corection factor.
bCalculations based on total sample weight with filter are entered on first line; calculations based on totali
.sample weight without filter are entered on second line for each stage.
Comments:
5-22
Form EED-070 C 6>79
-------
ACUREX
Corporation
ANDERSEN PARTICLE SIZE ANALYSIS
Plant.
Test Location-
Run No._^
Tare Weights:
Date _Z/^
Ry
Flow Rate
Location.
/7r
Final Weights:
Date
By-
Location.
STAGE
NO.
FILTER
NO.
FINAL
WT
(9)
TARE
WT
(9)
SAMPLE
WT
(9)a
% OF
TOTAL
CUMULATIVE
% OF TOTAL
Dp
/Mo
(/0J-20-1.
775
/til 23 6
/, in 6
5".
5V-
/',
#-00076
(.2-1 / 6 f
£2.
TOTAL WITH FILTER
TOTAL WITHOUT FILTER
IS-
7 -a/^iW
Blank correction value
Blank correction value
Stages 0 through 7
Stage F (final filter)
alncludes appropriate blank corection factor.
''Calculations based on total sample weight with filter are entered on first line; calculations based on total
.sample weight without filter are entered on second line for each stage.
Comments:
5-23
Form EED-070 C 6 79
-------
Corporation
ANDERSEN PARTICLE SIZE ANALYSIS
Plant
Test
Run No
Flow Rate
Tare Weights:
By
I nratinn
'<-i
< /
-------
ACUREX
ANALYTICAL REPORT
Sample of:
Sample Date: _ 2-~'2.'2.-
-------
5.5 SULFUR OXIDES EMISSIONS FROM CONTROLLED CONDENSATION SYSTEM SAMPLES
5-26
-------
ISOKINETIC PERFORMANCE WORKSHEET & PARTICULATE CALCULATIONS
Plant (X"^t.ff4^t^ c^SffiL / Performed by
Date
Sample Location 5//S-<<
Test No./Type
Barometric Pressure (in
Meter volume (std),
17 54 1 M I ( .
\(/.00) 1 \ ((
Hg)
«(i)(V*)
» i)
£U2 + 46° /
Volume of liquid collected (grams)
Volume of liquid at standard condition (scf)
Vlc x 0.04707
Stack gas proportion of
Vw std
water vapor
Vw std + Vm std Q£2.) + J&357
Molecular weight, stack
(Ib/lb-mole)
(% CQ2x 0.44) + (% Q2x
( x 0.44) + ( x.
Molecular weight, stack
(Tb/lb-mole)
Absolute stack pressure
p , Pstack gas dry
0.32) + (% N2+ % CO x 0.28)
0.32) + ( + x 0.28)
gas wet
(in. Hg)
oO) ( )
/ \ _i_
""""**,,.' 1^ fi
pb
\i
vm std
Vlc
vw std
wo
Md
Ms
'.
^7-W
»,n
<^(
j \^~**\
Or* O /
a-i
Fonn44O 3/84
5-27
-------
ISOKINETIC PERFORMANCE WORKSHEET & PARTICULATE CALCULATIONS
Plant (Zb*J«^ (JEEfi. J _ Performed by
Date
Sample Location
Test No. /Type
J2.
Barometric Pressure (in. Hg)
Meter volume (std),
"«m/v^\
\ "/ \Tm + 46° /
/g^/&a* !$*>\
17 fid I .11 ! * J
\$^)/y&J2) + 46° /
Volume of liquid collected (grams)
Volume of liquid at standard condition (scf)
Vlc x 0.04707
Stack gas proportion of water vapor
Vw std , @&
Vw std + Vm std &£^ + %£&
Molecular weight, stack gas dry
(Ib/lb-mole)
(% C02x 0.44) + (X 02x 0.32) + (% N2+ % CO x 0.28)
( x 0.44) + ( x 0.32) + ( + x 0.28)
Molecular weight, stack gas wet
(Ib/lb-mole)
Md(l-Bwo) + 18(BWQ), ( )(1- ) + 18( )
Absolute stack pressure (in. Hg)
' Pstack (in" H20) < >
p + szacK e. / .
Kb 13.6 ' ( ' + T3.6
Pb
Vm std
Vlc
vw std
uin
Md
Ms
>"»
Ps
^.^
.^b.^r
(s6.
Kit
n f^
l*ts'D
1
Form 440 S/84
5-28
-------
ACUREX
ANALYTICAL REPORT
Sample
Sample Date:
Requested By:
I.D. Number: _
Analytical Method:
/
Dale Of Analysis
3 ~-y'/~~
Lab I.'D. Number
Component
Analytical Result
Unit
/0<7, I
O-
Analysis By*
5-29
Form EED082
-------
5.6 TRACE ELEMENT ANALYSES OF FUEL AND SASS SAMPLES
In the following, samples labeled fuel, test 1 and fuel, test 2 are
blind duplicate samples of the same material.
5-30
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919 SOUTH HIGHLAND AVE., SUITE 210-B, LOMBARD. ILLINOIS 60148 (312) 953-9300
ROBERT L. TAYLOR, Ph.D.
MANAGER
INSTRUMENTAL ANALYSIS DIVISION
PLEASE ADDRESS ALL CORRESPONDENCE TO:
490 ORCHARD ST., GOLDEN, CO 80401
OFFICE TEL. (303) 278-9521
SINCE i*oa
May 16,1984
Mr. Christopher Mann
Acurex Corporation
P.O. Box 7555
Mountain View, CA 94042
RE: IAD #97-P137-116-10
Subcontract #SW59159A
Release #15
Analytical Report
Ten samples were received for analysis on April 2, 1984.
were assigned our IAD identification #97-Pl37-116-10.
These samples
Trace element determinations using Spark Source Mass Spectrometry per
EPA level 1 protocol are reported in separate attached reports.
Arsenic and Antimony were determined on two of the samples using hy-
dride generation atomic absorption spectrophotometry. Mercury was deter-
mined on all ten samples using flameless cold vapor atomic absorption spec-
trophotometry. The results of these determinations are presented in Table
No. I and are reported in parts per million (ppm) by weight on an "as re-
ceived" basis.
Carbon and Hydrogen were determined on four samples by an external lab-
oratory. The results of these determinations are presented in Table No. II
and are reported in weight percent (Wt.%) on an "as received" basis.
5-31
OVER 40 BRANCH LABORATORIES STRATEGICALLY ^CATEO IN PRIN^CIPAL COAL MINING AREAS.
TIDEWATER AND GREAT LAKES PORTS, AND RIVER LOADING FACILITIES
Chtrtar Member
-------
Sample ID
901458 EOR Filter
901459 EOR Filter Blank
901454 EOR XAD-2
901475 EOR XAD-2 Blank
901463 EOR Impinger 1
901461 EOR Impinger 1 Blank
901440 EOR Fuel, Test 1
901441 EOR Fuel, Test 2
901464 EOR Impinger 2 and 3
901462 EOR Impinger 2 & 3 Blank
Table No. I
(.ppm by Wt.)
Arsenic (As)
0.012
0.005
Sample ID
901458 EOR Filter
901459 EOR Filter Blank
901440 EOR Fuel, Test 1
901441 EOR Fuel, Test 2
Carbon
Analytical Report
#97-P137-116-10
Page 2
Antimony (Sb)
£0.004
<0.004
* Reported in ppm by weight of the filter.
Table No. II
CWt.%-As Received)
0.14**
0.05**
85.67
85.91
** Reported in weight per cent of the filter.
Hydrogen
0.17**
0.02**
11.22
11.36
Mercury (Hg)
0.04*
£0.02*
0.52
£0.4
0.0031
0.0089
£0.4
£0.4
0.004
<0.002
If you have any questions concerning these results, please call
Harold A. Cohnell
Assistant Laboratory Manager
Robert L. Taylor, Ph.D.,(Jj2lnager
Instrumental Analysis Division
HAC/gh
COMMERCIAL TESTING & ENGINEERING CO.
Original Copy Watermarked
For Your Protection
F-466
5-32
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919 SOUTH HIGHLAND AVE., SUITE 2IO-B. LOMBARD, ILLINOIS 60148 AREA CODE 312 953-9300
INSTRUMENTAL ANALYSIS DIVISION. 490 ORCHARD STREET, GOLDEN, COLORADO 80401. PHONE: 303 278-9521
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
Date: May 16, 1984
Analyst: G. Meagher
P.O. No.: Subcontract SW59159A, Release # 15, Project #EE7734.82
Sample No.: 901440 SPARK SOURCE AAASS SPEaROGRAPHIC ANALYSIS IAD No.: 97-P137-116-70
EOR Fuel
Test 1
ELEMENT CONC.
Urani urn
Thori urn
Bismuth
Lead 0 . 6
Thallium
Mercury MR
Gold
Platinum **i
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
STD Internal Standard
NR Not Reported
All elements not detected <
MC Major Component >
INT Interference
CONCENTRATION
ELEMENT CONC.
Terbium
Gadolinium
Europi urn
Samari urn
Neodymi urn
Praseodymi urn
Cerium
Lanthanum
Barium 0.8
Cesium
Iodine 0.5
Tel 1 uri urn
Antimony
Tin
Indium STD
Cadmi urn
Silver
Palladium
Rhodi urn
IN PPM WEIGHT
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsem c
Germanium
Gallium
Zinc
Copper
Nickel
Cobal t
Iron
Manganese
Chromi urn
*Heterogeneous
**Probable Contamination From
Sample Preparation /^~J
0.7 ppm Approved: \J^-J 1
100 ppm 9n
5-33
CONC. ELEMENT
Vanadium
*2 Titanium
0.09 Scandium
0.2 Calcium
0.06 Potassium
0.2 Chlorine
0.02 Sulfur
0.2 Phosphorus
0.5 Silicon
0.06 Aluminum
Magnesium
0.2 Sodium
2 Fluorine
0.7 Oxygen
6 Nitrogen
0.6 Carbon
10 Boron
0.4 Beryllium
0.4 Lithium
Hydrogen
Ut5t -U'r^E^
U Ac*tf Jptfv'
CONC.
6
3
<0.09
13
5
*MC
MC
4
19
9
8
10
=27
NR
NR
NR
0.2
0.5
NR
%
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919 SOUTH HIGHLAND AVE., SUITE 210-B, LOMBARD. ILLINOIS 60148 AREA CODE 312 953-9300
INSTRUMENTAL ANALYSIS DIVISION, 490 ORCHARD STREET. GOLDEN, COLORADO 80401. PHONE: 303 278-9521
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
P.O. No.: Subcontract SW59159A, Release #15, Project #EE7734.82
Sample No.: 901441 SPARK SOURCE AAASS SPECTROGRAPHIC ANALYSIS
EOR Fuel
Test 2 CONCENTRATION IN PPM WEIGHT
Date: May 16, 1984
Analyst: G. Meagher
IADNo.:97-P137-116-10
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead 0.5
Thai 1 i urn
Mercury NR
Gold-
Platinum
Iridium
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbi urn
Thulium
Erbium
Hoi mi urn
Dysprosium
ELEMENT CONC.
Terbi urn
Gadolinium
Europi urn
Samarium
Neodymi urn
Praseodymi urn
Cerium
Lanthanum
Barium 0.3
Cesium
Iodine 0.5
Tel 1 uri urn
Antimony
Tin
Indium STD
Cadmi urn
Silver
Palladium
Rhodi urn
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttri urn
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobal t
Iron
Manganese
Chromium
CONC.
0.3
0.03
0.06
0.04
0.2
0.06
0.4
0.05
£0.02
0.2
2
0.7
20
0.2
5
0:3
0.4
ELEMENT
Vanadium
Titanium
Scandi urn
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Ni trogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
CONC.
2
4
£0.03
5
3
19
MC
2
9
I
5
MC
=4
NR
NR
NR
0;08
<0.01
0.2
NR
STD Internal Standard
NR Not Reported
All elements not detected <
AAC Major Component >
INT Interference
0.02 ppm
100 ppm
Approved:
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919 SOUTH HIGHLAND AVE.. SUITE 210-B, LOMBARD. ILLINOIS 60148 AREA CODE 312 953-9300
INSTRUMENTAL ANALYSIS DIVISION, 490ORCHARD STREET. GOLDEN, COLORADO 80401, PHONE: 303 278-9521
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
Date: may 16, 1984
Analyst: 6. Meagher
P.O. No.: Subcontract SW59159A Release 15 Project 7601
Sample No.: 90145'8 SPARK SOURCE MASS SPECTROGRAPHIC ANALYSIS IAD No-= 97-P137-116-10
1 8r CONCENTRATION IN PPM WEIGHT of the Filter
ELEMENT
Urani urn
Thori urn
Bismuth
Lead
Thallium
Mercury
Gold
Platinum
Iridium
Osmi urn
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thul i urn
Erbium
Hoi mi urn
Dysprosium
STD Internal
CONC.
1
8
0.2
3
0.4
NR
0.4
2
0.4
1
0.4
2
2
4
Standard
NR - Not Reported
All elements not detected <
Mf Mxinr fnmnonent 5
ELEMENT CONC.
Terbi urn
Gadolinium
Europium
Samari urn
Neodymi urn
Praseodymi urn
Cerium
Lanthanum
Barium
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmi urn
Silver
Palladium
Rhodi urn
0.1 ppm
4000 ocm
0.8
4
0.4
4
12
4
12
16
36
0.4
0.8
3
8
4
STD
0.2
1
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttri urn
Strontium
Rubidium
Bromi ne
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromium
Os
Approved: ^ C-o
5-35
CONC.
12
0.8
3
24
16
0.8
8
4
16
2
12
64
8
MC
56
MC
20
36
1 ^4-
U*St'
//. 1
ELEMENT
Vanadium
Titanium
Scandi urn
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Nitrogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
-
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFnCES:1919SOUTHHIGHLANDAVE.,SUITE210.B, LOMBARD, ILLINOIS 60148 AREA CODE 312953-9300
INSTRUMENTAL ANALYSIS DIVISION. 490 ORCHARD STREET, GOLDEN, COLORADO 80401, PHONE: 303 278-9521
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
Date: May 16, 1984
Analyst: G. Meagher
P.O. No.: Subcontract SW59159A Release 15 Project 7601
Sample No.: 9Q1459 SPARK SOURCE AAASS SPECTROGRAPHIC ANALYSIS IAD No.:97-P137-116-10
EOR Filter Blank CONCENTRATION IN PPM WEIGHT of the Filter
ELEMENT CONC.
Urani urn
Thorium
Bismuth
Lead
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmi urn
Rheni urn
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium 8.
Hoi mi urn
ELEMENT
Terbium
Gadolinium
Europium
Samarium
Neodymi urn
Praseodymi urn
Cerium
Lanthanum
Bari urn
Cesium
Iodine
Tellurium
Antimony
Tin
Indium
Cadmi urn
Silver
Palladium
Rhodi urn
Dysprosium
STD Internal Standard
NR - Not Reported
All elements not detected < 0.2 ppm
MC Major Component >1000 ppm
CONC. ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
0.2 Strontium
0.1 Rubidium
0.2 Bromine
28 Selenium
Arsenic
0.2 Germanium
Gallium
Zinc
Copper
STD Nickel
±0.3 Cobalt
Iron
Manganese
Chromium
Approved: \(-
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: I919SOUTH HIGHLAND AVE., SUITE 210-B. LOMBARD, ILLINOIS 60148 AREA CODE 312 953-9300
INSTRUMENTAL ANALYSIS DIVISION, 490 ORCHARD STREET, GOLDEN. COLORADO 80401, PHONE: 303 278-9521
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
Date: May 16, 1984
Analyst: 6. Meagher
P.O. No.: Subcontract SW59159A, Release # 15, Project #EE7734.82
Sample No.: 901454 SPARK SOURCE MASS SPECTROGRAPHIC ANALYSIS 'AD No.: 97-P137-116-10
EOR XAD-2
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead 0.4
Thallium
Mercury NR
Gold
Platinum *0.6
Iridium
Osmi urn
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samari urn
Neodymi urn
Praseodymi urn
Cerium
Lanthanum
Barium 0.9
Cesium
Iodine 0.1
Tellurium
Antimony
Tin
Indium STD
Cadmium
Silver
Palladium
Rhodi urn
*Probable Contamination
Sample Preparation
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttri urn
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobal t
Iron
Manganese
Chromium
From
CONC.
0.8
0.1
0.2
0.07
0.05
0.08
3
0.4
0.6
0.04
5
0.4
0.4
ELEMENT
Vanadium
Titanium
Scandi urn
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Ni trogen
Carbon
Boron
Beryl 1 i urn
Lithium
Hydrogen
CONC.
0.09
4
0.2
17
12
4
6
2
13
1
9
3
*
NR
NR
NR
0.7
0.3
NR
STD Internal Standard
NR Not Reported
All elements not detected <
MC Major Component >
INT Interference
0.08 ppm
100 ppm
Approved:
5--
/6yU-
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919SOUTH HIGHLAND AVE.. SUITE 210-8. LOMBARD. ILLINOIS 60148 AREA CODE312 953-9300
INSTRUMENTAL ANALYSIS DIVISION, 490ORCHARD STREET, GOLDEN, COLORADO 80401, PHONE: 303 278-9521
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
Date: May 16, 1984
Analyst.- Q. Meagher
P.O. No.: Subcontract SW59159A, Release # 15, Project #EE7734.82
Sample No.: 901475 SPARK SOURCE MASS SPECTROGRAPHIC ANALYSIS IAD No-: 97-P137-116-10
EOR XAD-2 Blank
CONCENTRATION IN PPM WEIGHT
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead
Thallium
Mercury NR
Gold
Platinum **0.3
Iridium
Osmi urn
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbi urn
Thul i urn
Erbium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samari urn
Neodymium
Praseodymium
Cerium
Lanthanum
Barium 0.5
Cesium
Iodine 0.09
Tel 1 uri urn
Antimony
Tin
Indium STD
Cadmi urn 0.1
Silver
Palladium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobal t
Iron
Manganese
CONC. ELEMENT
Vanadium
0.7 Titanium
Scandi urn
0.1 Calcium
Potassium
0.09 Chlorine
Sulfur
Phosphorus
Silicon
0-04 Aluminum
<0.04 Magnesium
0.08 Sodium
O-7 Fluorine
0 - 6 Oxygen
0.5 Nitrogen
£0.07 carbon
6 Boron
0.3 Beryllium
Holmium Rhodium Chromium 0.5 Lithium
*Heterogeneous
Dysprosium **ProBable Contamination From Hydrogen
STD - internal standard Sample Preparation _ ^^^
NR - Not Reported { ) X7 «-rf ft \^t~,
All element not detected < 0.04 ppm Approved: VVOv 6-«O< U- C^2^
MC - Major Component > 100 ppm gh ^^"^ I , . x
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: I919SOUTH HIGHLANOAVE.. SUITE 210-8. LOMBARD, ILLINOIS 60)48 AREA CODE 312 953-9300
INSTRUMENTAL ANALYSIS DIVISION. 490 ORCHARD STREET, GOLDEN. COLORADO 80401. PHONE: 303 278-9521
To-. Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
P.O. No.: Subcontract SW59159A, Release # 15, Project #EE7734.82
Sample No.: XAD-2 SPARK SOURCE MASS SPECTROGRAPHIC ANALYSIS
Preparation Reagent Blank CONCENTRAT1ON IN PPAA WE1GHT
Date: May 16, 1984
Analyst: 6. Meagher
IAD No-= 97-P137-116-10
ELEMENT CONC.
Uranium ^0.4
Thorium 0.8
Bismuth
Lead 1
Thallium
Mercury NR
Gold **2
Platinum
Iri di urn
Osmium
Rhenium
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samarium
Neodymi urn 0.6
Praseodymi urn 0.4
Cerium 1
Lanthanum 1-
Barium 0.6
Cesium
Iodine 0.06
Tellurium
Antimony
Tin
Indium STD
Cadmi urn
Silver 0-2
Palladium
ELEMENT
Ruthenium
Molybdenum
Niobium
Zirconium
Yttri urn
Strontium
Rubidium
Bromi ne
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobal t
Iron
Manganese
Rhodium Chromium
heterogeneous
**Probable Contamination
STD Internal Standard
NR - Not Reported n n/.
All elementj not detected < «"* PP1"
MC - Major Component > 100 ppm
INT Interference
Approved: \^<£&
5-39
CONC.
<0.2
0.4
0.2
0.2
0.1
0.02
0.2
4
1
0.6
0.06
18
0.2
0.2
U5t\
ELEMENT
Vanadium
Titanium
Scandi urn
Calcium
Potassium
Chlorine
Sulfur
Phosphorus
Silicon
Aluminum
Magnesium
Sodium
Fluorine
Oxygen
Ni trogen
Carbon
Boron
Beryllium
Lithium
Hydrogen
J^tu^
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919 SOUTH HIGHLAND AVE., SUITE 210-B. LOMBARD, ILLINOIS 60148 AREA CODE 312 953-9300
INSTRUMENTAL ANALYSIS DIVISION. 490 ORCHARD STREET, GOLDEN. COLORADO 80401, PHONE: 303 278-9521
SINCt »
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
P.O. No.: Subcontract SW59159A, Release #15, Project #EE7734.82
Sample No.: 901463 SPARK SOURCE MASS SPECTROGRAPHIC ANALYSIS
EOR
Impinger 1 CONCENTRATION IN yg/mL
Date: May 16, 1984
Analyst: G. Meagher
IAD No-= 97-P137-116-10
ELEMENT CONC.
Uranium
Thorium
Bismuth
Lead 6
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmi urn
Rheni urn
Tungsten
Tantalum
Hafnium
Lutetium
Ytterbium
Thulium
Erbium
Hoi mi urn
INT Interference
0.008 ug/mL
10 yg/mL
Approve*
-------
Reply to
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919SOUTH HIGHLANDAVE..SUITE210-B, LOMBARD, ILLINOIS 60148 AREA CODE 312 953-9300
INSTRUMENTAL ANALYSIS DIVISION, 490 ORCHARD STREET. GOLDEN, COLORADO BW01, PHONE: 303 278-9521
To: Acurex Corporation
555 Clyde Avenue
P.O. Box 7555
Mountain View, CA 94039
zft
P.O. No.: Subcontract SW59159A, Release #15, Project #EE7734.82
Sample No.: 901461 SPARK SOURCE AAASS SPECTROGRAPHIC ANALYSIS
EOR Impinger
1 Blank CONCENTRATION IN
Date: May 16, 1984
Analyst: Q. Meagher
IADNo.:97_pi37_ii6-10
ELEMENT CONC.
Uranium
Thori urn
Bismuth
Lead
Thallium
Mercury NR
Gold
Platinum
Iridium
Osmi urn
Rhenium
Tungsten
Tantalum
Hafnium
Luteti urn
Ytterbium
Thulium
Erbium
Hoi mi urn
Dysprosium
STD Internal Standard
NR - Not Reported
All elements not detected <
MC - Major Component >
ELEMENT CONC.
Terbium
Gadolinium
Europium
Samari urn
Neodymi urn
Praseodymium
Cerium
Lanthanum
Barium 0.02
Cesium
Iodine 0.03
Tellurium 0.006
Antimony £0.009
Tin 0.2
Indium STD
Cadmi urn
Silver
Palladium
Rhodi urn
heterogeneous
0.003 ng/mL
10 yg/mL
ELEMENT
Ruthenium
Molybdenum
Ni obi urn
Zirconium
Yttrium
Strontium
Rubidium
Bromine
Selenium
Arsenic
Germanium
Gallium
Zinc
Copper
Nickel
Cobalt
Iron
Manganese
Chromi urn
Approved: \^O
. .. 11
CONC. ELEMENT
Vanadium
0.03 Titanium
£0.004 Scandium
0.01 Calcium
Potassium
0.003 Chlorine
Sulfur
0.008 Phosphorus
0.006 Silicon
£0.002 Aluminum
£0.002 Magnesium
0.003 sodium
0.02 Fluorine
0.002 oxygen
0.01 Nitrogen
0.004 carbon
0 . 06 Boron
0.01 Beryllium
0.01 Lithium
Hydrogen
/Usfif«c3u^
(\t .. . V LI (]
CONC.
0.003
0.04
0.005
0.4
0.2
*6
MC
1
0.6
0.05
0.7
MC
=0.3
NR
NR
NR
0.002
0.01
NR
Q^
INT Interference
5-41
-------
COMMERCIAL TESTING & ENGINEERING CO.
GENERAL OFFICES: 1919 SOUTH HIGHLAND AV6.. SUITE 210-B, LOMBARD. ILLINOIS 6014S (312) 953-9300
GERALD T SKAR ~SH PLEASE ADDRESS ALL CORRESPONDENCE TO
«.K,.^CD' ^IW 490 ORCHARD ST.. GOLDEN, CO. 80401
MANAGER
.NSTRUMENTAL ANALYS.S D.V.SION
SINCE 1908
August 2, 1984
Mr. Larry Water! and
Acurex Corporation
P.O. Box 7555
Mountain View, CA 94039
RE: IAD #97-P897-116-06
Subcontract #SW 59159A
Release #16
Analytical Report
Six samples, previously analyzed for trace elements by spark
source mass spectrometry, under our IAD identification #97-P137-116-10,
were logged in under our IAD identification #97-P897-116-06 on July 16,
1984, for additional analysis.
Chlorine and fluorine were determined using specific ion electrode
methodology. Phosphorus was determined colorimetrically.
Depending on sample type and the amount of sample available, sulfur
was determined turbidimetrically or by X-ray fluorescence spectrometry.
The remaining elemental analysis was performed using flame atomic
absorption/emission spectrophotometry.
The results of these determinations are presented in the following
tables. Samples #1 and 2 are reported in total micrograms (ug) on the
filter. Samples #3 and 4 are reported in micrograms per millilitre
(pg/mL). Samples #5 and 6 are reported in micrograms per gram (yg/g).
All values are reported on an "as received" basis.
If you have any questions concerning these results, please call.
HAC/as
arold A. Connell
Project Coordinator
5_42 Chwtar MimlMr
OVER 40 BRANCH LABORATORIES STRATEGICALLY LOCATED IN PRINCIPAL COAL MINING AREAS.
TIDEWATER AND GREAT LAKES PORTS. AND RIVER LOADING FACILITIES
-------
Table No. I
(Total yg on the Filter)
Parameter
Aluminum, (Al)
Calcium, (Ca)
Chlorine, (Cl)
Iron, (Fe)
Potassium, (K)
Magnesium, (Mg)
Sodium, (Na)
Nickel, (Ni)
Phosphorus, (P)
Sulfur, (S)
Silicon, (Si)
Vanadium, (V)
#1 - 901458
EOR Filter
7,000
16,000
44,300
10,150
80
2,640
1,930
33,100
590
125
780
1,320
#2 901459
EOR Filter Blank
3,740
Table No. II
Parameter
Copper, (Cu)
Fluorine, (F)
Magnesium, (Mg)
Sodium, (Na)
Sulfur, (S)
Zinc, (Zn)
#3 - 901463
EOR Impinger 1
71.9
0.89
0.14
4,960
6,920
30
#4 - 901461
EOR Impinger 1 Blank
0.39
<50
Table No. Ill
Parameter
Chlorine, (Cl)
Sodium, (Na)
Sulfur, (S)
#5 - 901440
EOR Fuel. Test 1
25
132
11,700
#6 - 901441
EOR Fuel, Test 2
21
104
11,600
COMMERCIAL TESTING & ENGINEERING CO.
Original Copy Watermarked
For Your Protection
5-43
-------
5.7 ORGANIC ANALYSES OF SASS SAMPLES: TOTAL CHROMATOGRAPHABLE ORGANICS
(TCO), GRAVIMETRIC ORGANICS (GRAV), GAS CHROMATOGRAPHY MASS SPECTROMETRY
(GC/MS), and INFRARED (IR) SPECTRA OF TOTAL SAMPLE EXTRACTS
5-44
-------
f\ ACUREX
'carbazole, 7, 12-di methyl benzo (a) anthracene,
3-methylcholanthrene, and perylene were sought employing the
computerized library search and manual interpretation. The
assignment and quantitation o-f these organics is tentative since
analytical standards of these compounds were not available for
analysis. Benzo(c)phenanthrene, dibenzo(c,g>carbazole,
7-12-dimethylbenzo(a)anthracene, 3methylcholanthrene and perylene
were not detected in any of the samples at levels above 1OO ug
per train.
After extraction of the XAD field blank, the same resin was
spiked with 400 ug each of dodecane and hexadecane for TCO
analysis, 400 ug each of naphthalene, phenanthrene, and pyrene
for PAH analysis, and 10 mg of bis(2-ethylhexyl)phthalate which
combined with the phenanthrene and pyrene for the BRAV analysis.
Results are presented in Tables 1 through 3. Chromatograms and
spectra are attached.
Submitted by:
Greg N/coll Viorica Lopez-Avila, Ph.D.
Manag/ir, Inorganic Chemistry Technical Director
GN/VLA/ats
Attachments
555 Clyde Avenue, P.O. Box 7555. Mountain View. CA 94039 (415)964-3200 Telex: 34-6391 TWX: 910-7796593
-------
Acurex/ES
8402-006
Page 2 c-f 4
Table 1. TCO and GRAV Results
Samgl.e ID
Filters
XAD*
XAD blank
XAD spike
XAD spike level
XAD spike recovery
TCO
4.1 mg/train
O.34 mg/train
784 ug
BOO ug**
987.
<3 mg/train
6 mg/train
3 mg/train
11 mg
1O.8 mg***
102%
* Blank corrected
** 4OO ug each o-f C(12) and CU6)-alkanes
*** 10 mg o-f bis(2-ethylhexyl )phthalate, 4OO ug of phenanthrene,
and 4OO ug o-f pyrene
5-46
-------
Acurex/ES
8402-OO6
Page 3 o-f 4
Table 2. BC/MS Results, ug/train
Dibutylphthalate
Dimethylphthalate
Naphthalene
Phenanthrene
Phenol
Pyrene
Other Priority Pollutants
XAD
<50
1OO
4O
<10
20
<10
ND**
% Recovery
ked XAD of sgiked XAD
<5O
60
20
<1O
10
<10
ND
NS***
NS
42O
40O
NS
51O
NS
105
100
128
* Duplicate injection
** ND - Not detected
*** NS - Not spiked
5-47
-------
Acurex/ES
8402-006
Page 4 o-f 4
Table 3. Sample Disposition
Initial Subcontract
901455 #31
901456 #32
901457 #33
901458 #34
901459 #35
901453
9O1454
901475
901442
9O1443
9O1444
901463
901461
901464
9O1462
9O144O
Filter
Filter
Filter
Filter
Filter blank
OMR
XAD
XAD blank
XAD spike
OMC
Imp 1
I mp 1 b 1 an k
I mp 28<3
Imp 2&3 blank
Grab -fuel 1A
395 ml
130 g
130 g
125 g
1910 ml
595 ml_**
1 L
92O mL
1 L
5OO mL
327.
33%
28%
30'/.
10O7.
5 g
5 g
O
10O mL
1OO mL
10O mL
100 mL
100; 100;
100 mL
125 g
125 g
125 g
0
0
0
0
O
627.*
O
87"/.*
877.*
9O7.*
255O mL
1 L
82O mL
1 L
200 mL
* as extract
** Imp 1 8< OMC (aqueous) volume is 2650 mL
5-48
-------
IR REPORT
SAMPLE:
8402-006-1 Filters
to-'1)
Intimity
Anignmmt
Comments
No Peaks
5-49
-------
IR REPORT
SAMPLE:
8402-006-7 XAD
*~£fi~
2930
1732
1438
1255
1165
1115
t
Intimity
M
S
W
W
W
W
-
Anignmwit ConrnitnB
C-H Aliphatic
C=0
CH
C-0
C-0
C-0
..
/~
5-50
-------
R REPORT
SAMPLE:. 8402-006-8 XAD Blank
WaMMmtar
- to-*1)
2928
Intraity
S
Anignnwnt Comnwnti
C-H Aliphatic
Very weak spectrum
*
5-51
-------
IR REPORT
SAMPLE:
8402-006-9 XAD Spike
WmMwnfar
- to-'1)
2931
1728
1600
1759
1463
1381
1275
1123
1073
1040
744
t
Invraity
S
S
w
w
M
W
S
M
M
W
W
Anignnwnt Cemnwna
C-H Aliphatic
C=0
C=C Aromatic
C=C Aromatic
C-H Aliphatic
C-H Aliphatic
C-0
C-0
C-0
Unassigned
. CH '
»
5-52
-------
5.8 VOLATILE ORGANICS ANALYSES OF VOST TRAPS
Inhouse experiments regarding the level of precautions needed to prevent
blank trap contamination during storage and shipping were being performed
during the time period of these tests. As a consequence, six pairs of trap
blanks were available for use in this test: two pairs of trip blanks, two
pairs of field blanks, and two pairs of laboratory blanks, differing only in
the manner in which they were stored. As suggested by the VOST protocol, the
pair t-test was used to assess the "sameness" of each blank trap pair- Use
of this test showed all six blank pairs to be the same, with a confidence
.
level of 70 percent or greater- Therefore, a mean blank trap level for each
of the volatile compounds determined, with an associated standard deviation,
was used to blank-correct each sample trap analyzed. The concentration of a
compound had to be present in a sample trap at a level greater than three
standard deviations above the mean blank level to be considered actually
present in the flue gas sampled (as suggested by the VOST protocol). Based
on this criterion, only benzene, toluene, and ethyl benzene were found to be
present in sample traps at levels statistically different from blank traps.
Thus, only emissions of these three components are reported in Volume 1 of
this report.
The analytical data report follows. Traps denoted by the suffix "A" are
the Tenax/charcoal trap of a run pair.
5-53
-------
ACUREX
Corporation
Energy & Environmental Division
Acurex/ES (CMEA)
Attention: Larry Waterland/2-2260
March 9, 1984
Acurex ID*: 8402-004
Client POI: 307736.82
302865.65
Page 1 of 5
Subject: Analysis of 10 Pairs of Tenax Traps,
Received 2/2/84
The above referenced samples were Individually analyzed by GC/MS according to
EPA VOST Protocol for volatile organics (EPA Method 624 Priority Pollutants).
Sample Analysis results are listed in Table 1. Blank data and recovery data
from spiked Tenax traps are given in Tables 2 and 3, respectively.
If you have any questions, please call.
Prepared by:
(S.
William 6. Hellier
Staff Chemist
Approved by:
Viorica Lopez-Avila, Pn.D.
Technical Director
WGH/VLA/ats
555 Clyde Avenue. P.O. Box 7555. Mountain View. CA 94039 (415) 964-3200 ' Telex: 34-6391 TWX: 910-7796593
5-54
-------
Table 1. Results of Volatile Organic Analyses
]
' Ol
g"
,
Sample ID
Trap #
Priority Pollutants
Chi oromethane
Dlchloromethane
1 ,1-Dichloroethylene
Trans-1 ,2-Oichloroethylene
Chloroform
1,2-Dichloroethane
1 ,1 ,1-Trichloroethane
Carbon tetrachloride
1 ,2-D1chloropropane
Tri chl oroethyl ene
1 ,1 ,2-Trichloroe thane
Benzene
Tetrachl oroethyl ene
1 ,1 ,2,2-Tetrachloroethane
Toluene
Chlorobenzene
Ethyl benzene
Nonprlority Pollutants
Xylenes
Detection Limit
Percent Surrogate Recovery
Tol uene-dg
Concentration (ng/trap)
Run #4
7a
302
137
ND
2
28
3
9
77
4
8
29
63
5
47
67
10
8
11
2
65
Run #4
33Aa
4900
2670
ND
ND
ND
ND
19
ND
ND
3
ND
35
ND
ND
42
ND
6
9
2
86
Field
Blank
40a
2260
550
ND
ND
ND
ND
10
ND
ND
ND
ND
10
ND
ND
7
ND
2
4
2
13C
Field
Blank
7Aa
27
3050
ND
ND
ND
ND
7
ND
ND
12
ND
38
ND
ND
35
ND
29
30
2
146
Trip
Blank
42a
523
396
ND
ND
ND
ND
9
12
ND
11
30
38
ND
ND
29
ND
ND
8
2
219
Trip
Blank
15Aa
58
4160
8
ND
12
24
ND
8
22
ND
29
51
ND
10
16
12
ND
15
2
100
Run §2
23
960
103
ND
ND
24
ND
8
ND
4
ND
ND
850
' ND
ND
33
ND
1
7
1
79
Run n
24Ab
87
933
6
ND
ND
ND
ND
5
ND
ND
ND
34
ND
6
52
4
ND
10
1
136
Lab
Blank
8
290
115
ND
ND
35
ND
7
ND
ND
ND
ND
14
ND
ND
13
ND
1
5
1
80
Lab
Blank
10A
53
225
ND
3
ND
ND
3
5
ND
ND
ND
ND
ND
11
. 52
ND
ND
15
1
107
a - Shipped in wooden boxes
b - Transport tube received broken
c - Low recovery of Internal standards
ND - Not detected
-o oo S»
a> 4> o
to o c
CD IS) "J
i m
ro o x
o ^
o 4* m
HI «/>
in
-------
Table 1. Results of Volatile Organic Analyses (Cont.)
Sample ID
Trap #
Priority Pollutants
Chloromethane
Vinyl Chloride
Dichloromethane
l,l-D1chloroethylene
Trans- 1 ,2-D1chloroethylene
Chloroform
1,2-Dlchloroethane
1,1.,1-Trlchloroethane
Carbon Tetrachlorlde
1.2-Dlchloropropane
TMchloroethylene
1,1,2-THchloroethane
Benzene
Tetrachloroethylene
1,1,2,2-Tetrachloroethane
Toluene
Ethyl benzene
Manor tor 1ty Pollutants
Styrene
Xy lanes
'Detection Limit
Percent Surrogate Recovery
Toluene-dg
Concentration (ng/trap)
Glass
Sealed
44
830
NO
120
ND
ND
ND
ND
ND
ND
ND
ND
ND
19
ND
ND
10
3
1
2
1
108
Glass
Sealed
20A
37
ND
121
10
ND
ND
12
15
8
ND
ND
ND
5
17
8
42
9
ND
ND
1
134
Run #1
45
519
ND
109
ND
ND
24
8
30
ND
27
8
ND
2640
11
ND
144
9
2
8
2
91
Run #1
19A
146
9
25200
3
3
ND
ND
ND
ND
17
6
54
ND
32
ND
2
72
6
ND
2
21 3C
Run #3
21a,b
2240
ND
63
ND
ND
ND
ND
8
46
ND
ND
ND
205
ND
ND
57
4
ND
6
2
95
Run #3
13b
66
ND
889
ND
ND
ND
ND
10
ND
ND
ND
ND
46
21
ND
34
5
ND
10
2
142
Field
Blank
11
721
ND
115
ND
ND
3
ND
ND
ND
ND
5
ND
26
ND
ND
2
ND
ND
4
2
111
Field
Blank
32A
28
ND
1550
ND
ND
ND
ND
3
ND
ND
ND
ND
1
4
3
2
2
ND
7
2
103
Trip
Blank
9
1340
ND
118
22
ND
ND
ND
20
ND
ND
ND
ND
20
ND
ND
9
4
3
3
\
2
106
Trip
Blank
35A
71
ND
204
ND
ND
3
ND
10
ND
ND
ND
ND
41
ND
8
44
7
6
9
2
142
a - Transport tube received broken
b -Transported with activated charcoal
c - Low recovery of internal standards
ND - Not Detected
-a oo j»
01 4*0
to oc
i n
w o x^
o *» m
-h to
-------
Table 2. Analysis Blanks
Sample ID
Date
Priority Pollutants
Chloromethane
D1 chl or ome thane
1,1-Dtchloroethylene
1 ,2-D1chloroethane
1 ,1 ,l-Tr1chloroethane
Trtchloroethylene
Chl orodl bromomethane
1 ,1 ,2-Trichloroethane
Benzene
Tetrachloroethylene
1,1,2,2-Tetrachloroethane
Toluene
Chlorobenzene
Ethyl benzene
Nonprlorlty Pollutants
Styrene
Xylenes
Detection Limit
Percent Surrogate Recovery
Tol uene-dg
Concentration (ng/Trap)
Purge
Blank
2/2/84
70
78
ND
ND
ND
4
ND
ND
18
2
6
4
ND
3
3
4
2
100
Trap
Blank
2/2/84
286
60
14
7
59
23
ND
10
41
3
13
12
ND
3
2
5
2
95
Purge
Blank
2/3/84
4
(81
ND
ND
ND
ND
ND
ND
14
ND
ND
3
ND
3
ND
5
2
93
Trap
Blank
2/3/84
315
68
ND
ND
ND
2
ND
6
18
21
23
10
7
8
7
9
2
91
Purge
Blank
2/5/84
17
49
ND
ND
ND
ND
ND
ND
12
ND
ND
5
ND
1
ND
ND
2
96
Trap
Blank
2/5/84
2130
62
ND
ND
ND
ND
15
24
26
ND
41
12
ND
9
3
ND
2
102
Purge
Blank
2/6/84
63
115
NO
ND
ND
ND
ND
ND
2
ND
ND
ND
ND
ND
5
52
2
104
Trap
Blank
2/6/84
64
59
ND
11
ND
ND
ND
ND
19
ND
ND
12
ND
7
10
10
2
109
en
en
ND - Not detected
o oo >»
e> -P» o
iO O C
n> ro -j
m
en
-------
Table 3. Tenax Trap Spike Recovery
Acurex/ES
8402-004
Page 5 of 5
Sample ID
Date
Chloromethane
Bromome thane
Vinyl chloride
Chloroethane
Dichloromethane
1,1-Dichloroethylene
1 ,1-Di Chloroethane
Trans-1 ,2-Dichloroethylene
Chloroform
1 ,2-Di Chloroethane
1 ,1 ,1-Trichloroethane
Carbon tetrachloride
Dichlorobromomethane
1 ,2-Dichloropropane
Trichl oroethylene
1,1 ,2-Trichloroethane
Benrsne
Tetrachl oroethyl ene
Tol uene
Chlorobenzene
Ethyl benzene
Nonpriority Pollutants
Xylenes
Percent Surrogate Recovery
Tol uene-dg
% Recovery
200 ng
Trap
2/2/84
404
116
112
116
116
131
128
130
130
54
118
118
100
93
"90
39
118
100
106
66
85
66
104
200 ng
Trap
2/3/84
615
160
163
170
136
171
161
170
154
87
158
161
95
65
66
54
96
,78
67
31
38
42
72
200 ng
Trap
2/5/84
338
114
117
100
109
112
114
114
no
82
108
no
91
96
101
113
138
102
no
68
81
54
105
200 ng
Trap
2/6/84
49
90
74
70
106
73
84
78
88
70
78
60
68
139
111
58
152
84
91
43
44
54
95
5-58
-------
5.9 N20 EMISSIONS BY GC/ECD
5-59
-------
ACUREX.
Corporation
Energy & Environmental Division
Acurex/ES
Attention: Larry Water!and
May 21, 1984
Acurex ID#: 8404-025
Client P0#: 307736.82
Page 1 of 1
Subject: Analysis of 3 Gas Bombs for Nitrous Oxide by 6C/ECD
The above referenced samples were analyzed by GC/ECD according to previously
reported method.
Results are listed in the table below:
Sample ID
(ppm)
901428
901448
901470
<0.5*
2
n
* Sample cylinder was not pressurized
sample may have leaked.
If you have any questions, please call.
Prepared by:
William G. HelTier
Staff Chemist
Approved by:
Viorica Lopez-Avila, Ph.D.
Technical Director
WGH/VLA/ats
555 Clyde Avenue, P.O. Box 7555, Mountain View. CA 94039 (415) 964-3200 Telex: 34-6391 TWX: 910-7796593
5-60
-------
5.10 NOX EMISSIONS BY EPA METHOD 7
Laboratory analysis data for the Method 7 test performed on
January 24, 1984, was Included on the forms reporting the sampling and
recovery data included in Section 4.2. Analysis data for the tests performed
on February 8 and 24, 1984, appear on the following pages.
5-61
-------
ACUREX
ANALYTICAL REPORT
Sample
»f. Cfl&l/G&Z
Sample Date:.
/
2-
Requested By:
I.D. Number
Analytical Method:
Date of Analysis:
*7
A) * L ^
: ^A
Lab l.D. Number
Analytical Result
Unrt
r
7
2,2.^,0
it
37 1
/
1*3,2
5-62
Analysts By.
Date
U-i3
FarmEEO-M?
-------
ACUREX
ANALYTICAL REPORT
Sample of:
Sample Date;_Z__r_
Requested By: <*?/»"*}
I.D. Number
Analytical Method:
/
Date Of Anatysis-
"
-------
ACUREX
ANALYTICAL REPORT
Sample
M. C/l&l/eeK
Sample Date:.
Requested By:
I.D. Number
? 77S 5s
Analytical
Date of Analyst
I Unit
LMJ/J^/
\ /
Lab I.O. Number
Analyt
cal Result
J"
7
/o
/J/,
73,
Analysis By.
5-64
Date.
^
^
*/*
-------
TECHNICAL REPORT DATA
(Please read Inunctions on the reverse before completing}
REPORT NO.
EPA-600/7-86-013b
3. RECIPIENT'S ACCESSION NO.
.TITLE AND SUBTITLE
Environmental Assessment of an Enhanced Oil
Recovery Steam Generator Equipped with an EPA
Heavy-oil Low-NOx Burner; Volume II*
6. REPORT OAT6
April 1986
6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S) "
C. Castaldini, L. R. Water-land, and R. De Rosier
8. PERFORMING ORGANIZATION REPORT NO
9. PERFORMING ORGANIZATION NAME AND ADDRESS
Acurex Corporation
Energy and Environmental Division
P. O. Box 7044
Mountain View, California 94039
10. PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-02-3188
12. SPONSORING AGENCY NAME AND ADDRESS
EPA, Office of Research and Development
Air and Energy Engineering Research Laboratory
Research Triangle Park, NC 27711
13. TYPE OF REPORT AND PERIOD COVERED
Final; 1/84 - 1/85
14. SPONSORING AGENCY CODE
EPA/600/13
is. SUPPLEMENTARY NOTES AKERL prO|ject officer is Joseph A. McSorley, Mail Drop 65. 919 /
541-2920. Volume I contains technical results. (*) Volume II is Data Supplement.
ID. ABSTRACT
The report gives results of comprehensive emission measurements and
30-day flue gas monitoring on a 16-MW (55 million Btu/hr) enhanced oil recovery
steam generator equipped with the EPA low-NOx burner firing high-nitrogen crude.
The 1-day comprehensive measurements included quantification of semivolatile or-
ganics and 73 trace elements; volatile organic sampling train quantisation of volatile
organic priority pollutants; EPA Method 5/8 for particulate and SOx; controlled con-
densation for SOx; Andersen impactors for particle size distribution; grab samples
for N2O; and continuous flue gas monitoring. NOx emissions averaged 70 ppm at 3%
O2, well below the target of 85 ppm. CO emissions were below 30 ppm/ and SO2
averaged about 550 ppm. Solid particulates were emitted at about 27 ng/J (96 mg/
dscm); condensible particulates were about half that. Volatile organics (benzene,
toluene, and ethylbenzene) were measured in the 0.4 to 20 ppb range. Semivolatile
organics (naphthalene and phenol) were detected at about 0.3 ppb. Subsequent contin-
uous monitoring of flue gas criteria emissions showed NOx below 80 ppm at 3% O2
with an average of 70 ppm. CO emissions were generally less than 30 ppm.
7.
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
b.lOENTIFIERS/OPEN ENDED TERMS
c. COSATI Field/Group
Pollution
Assessments
Boilers
Oil Recovery
Crude Oil
Combustion
Pollution Control
Stationary Sources
Environmental Assess-
ment
Low-NOx Burners
13B
14B
ISA
081,11H
21B
3. DISTRIBUTION STATEMENT
Release to Public
19. SECURITY CLASS (This Report)
Unclass ified
21..NO. OF PAGES
187~
20. SECURITY CLASS (This page)
Unclassified
22. PRICE
CPA Form 2320-1 («-73J
5-65
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