EPA-650/2-74-031-a
April  1974
                           Environmental Protection Technology Series



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                             EPA-650/2-74-031-0
 APPLICATION  OF  HOLOGRAPHIC
METHODS TO THE  MEASUREMENT
  OF FLAMES  AND  PARTICIPATE,
              VOLUME  I
                   by

           A .B . Witte and D .E. Haflinger

              TRW Systems Group
               One Space Park
          Redondo Beach, California 90278
             Contract No. 68-02-0603
              ROAP No. 21ADG-51
           Program Element No. 1AB014
        Project Officer: William B. Kuykendal
           Control Systems Laboratory
        National Environmental Research Center
        Research Triangle Park, N. C. 27711
                Prepared for

       OFFICE OF RESEARCH AND DEVELOPMENT
       ENVIRONMENTAL PROTECTION AGENCY
            WASHINGTON, D.C. 20460

                 April 1974

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This report has been reviewed by the Environmental Protection Agency
and approved for publication.  Approval does not signify that the
contents necessarily reflect the views and policies of the Agency,
nor does mention of trade names or commercial products constitute
endorsement or recommendation for use.
                                  11

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                         TRW REPORT NO. 23523-6001-TU-00
  APPLICATION OF HOLOGRAPHIC METHODS

                TO THE

MEASUREMENT OF FLAMES AND PARTICIPATE
               VOLUME I
             Prepared for

  OFFICE OF RESEARCH AND DEVELOPMENT
   ENVIRONMENTAL PROTECTION AGENCY

        Washington, D.C. 20460
                  111

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                                ABSTRACT

     The report gives results of the application of a pulsed ruby laser
holographic interferometer to the study of flames, in hopes of extracting
temperature profile data.  The principle involved is to record holograph-
ically the interferogram which presents a three-dimensional record of the
interference fringe pattern.  The density profile and hence the temperature
profile can be calculated from the fringe shift information.  The report
presents data for a methane-air burner operating both as a diffusion flame
and as a premixed flame.  The large number of fringe shifts recorded on an
interferogram complicated the reduction of the methane-air data, but it was
possible to correlate the interferometrically derived temperature data with
thermocouple measurements.  Application of the technique to a 0.2 gal/hr oil
burner was unsuccessful  because the highly turbulent flame caused an inter-
ference pattern that could not be deciphered.  This report was submitted in
fulfillment of TRW Project No. 23523 and Contract No. 68-02-0603 by TRW
Systems Group under the  sponsorship of the Environmental Protection Agency.
Work was completed as of November 1973.
                                     IV

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                              CONTENTS
                                                                Page
1.   INTRODUCTION	   1
2.   EXPERIMENTAL APPARATUS	   3
     2.1  Hauck Burner 	   3
     2.2  Methane-Air Burner 	   4
     2.3  Holocamera	   5
3.   TEST PROCEDURE.	   7
4.   DATA REDUCTION PROCEDURE	   9
                         _ i
     4.1  Introduction . -;	   9
     4.2  Abel Inversion Technique	;	   9
     4.3  Comparison Model  to Account for Scene Difference ...   10
     4.4  Premixed Flame Fringe Shift Equation 	   11
     4.5  Diffusion Flame Fringe Shift Equation	12
     4.6  Density Calculation Procedure	15
     4.7  Sample Calculations	  .   16
     4.8  Excess Air Effect	17
     4.9  Velocity Ratio and Reynolds Number 	   18
5.   RESULTS.	21
     5.1  Sequence of Progress and Problems Solved  	   21
     5.2  Hauck Burner	22
     5.3  Flame Interferometry 	   22
     5.4  Premixed Methane-Air Flame 	   22
     5.5  Diffusion Methane-Air FUme	35
6.   CONCLUSIONS AND RECOMMENDATIONS 	   56
     6.1  Conclusions	56
          6.1.1  Interferometric Data Reduction Procedures ...   56
          6.1.2  Diffusion  Flame	56
          6.1.3  Premixed Flame.	57
          6.1.4  Oil Burners	57
     6.2  Recommendations	57
REFERENCES	58

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                            ILLUSTRATIONS
                                                                 Page
2-1    Sectional  View of Hauck Proportioning Oil  Burner

2-2
2-3
2-4
4-1
4-2

4-3

4-4
5-1

5-2

5-3

5-4

5-5

5-6

5-7

5-8
5-9
5-10
5-11

and Magnified View of Nozzle Section 	
Methane-Air Burner 	
Air-Methane Premix Fitting 	
Schematic of Holocamera 	
Diagram of Light Beam 	
Molecular Weight Versus Excess Air for Methane-Air
Combustion 	 . . . .
Glades tone- Dale Constant Versus Excess Air for
Methane-Air Combustion 	
Methane-Air Burner with Annul us Insert 	
Infinite Fringe Interferogram of Methane-Air Burner
With Chimney 	
Finite Fringe Interferogram of Methane-Air Burner
With Chimney 	
Infinite Fringe Interferogram of Methane-Air Burner
Without Chimney 	
Finite Fringe Interferogram of Methane-Air Burner
Without Chimney 	
Interferogram of Pre-Mixed Flame With Condition
Shown in Table 5-1 	
Interferogram of Pre-Mixed Flame With Condition
Shown in Table 5-1 	
Comparison Between Equations (4-5) and (4-6) for
Interferogram Data EPA No. 5-5 	
Fringe Shift for Interferogram No. 5-5. . 	
Density Solution for Interferogram EPA No. 5-6 	
Fringe Shift for Interferogram EPA No. 5-6 	
Effect of Excess Air on Density Profiles for
Interferogram No. 5-6 	
3
4
5
6
14

18

19
20

23

23

24

24

25

25

27
28
29
30

31
                                   vi

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                       ILLUSTRATIONS (Continued)
5-12   Test Interferogram for Rectangular Box with
       Pyrex Windows	    32
5-13   Effect of Wall  Temperature on Density Profile for
       Interferogram No. 5-6	    33
5-14   Interferogram with Thermocouples Attached	    34
5-15   Temperature of Methane Air Premixed Flame Versus Percent
       Excess Air Assumed 	    36
5-16   Partial Pressures of Combustion Products 	    37
5-17   Density Profile for Interferogram No. 5-14 With
       14 Percent Excess Air.	    40
5-18   Schematic of Typical Fringe Pattern Divided Into Its
       Three Compositional Regions	    42
5-19   Reconstructed Interferogram	    42
5-20   Reconstructed Interferogram	    43
5-21   Reconstructed Interferogram	    43
5-22   Reconstructed Interferogram	    43
5-23   Reconstructed Interferogram	    43
5-24   Reconstructed Interferogram	    43
5-25   Reconstructed Interferogram	    44
5-26   Reconstructed Interferogram	    44
                                 J
5-27   Reconstructed Interferogram	    44
5-28   Reconstructed Interferogram	,	    44
5-29   Reconstructed Interferogram	, .  .    44
5-30   Reconstructed Interferogram	    46
5-31   Reconstructed Interferogram	    46
5-»32   Reconstructed Interferogram	    46
5-33   Reconstructed Interferogram	    46
                                  vii

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                       ILLUSTRATIONS (Continued)
                                                                 Page
5-34   Reconstructed Interferogram	   46
5-35   Reconstructed Interferogram	   47
5-36   Reconstructed Interferogram	   47
5-37   Reconstructed Interferogram	   47
5-38   Reconstructed Interferogram	   47
5-39   Reconstructed Interferogram	   47
5-40   Plot of Peak Temperatures of Reduced Interferograms
       and Thermocouple Data	   49
5-41   Temperatures Profiles With r   0.825 inch, Varying
       Reynolds Number, Constant UA/UF	   50
5-42   Temperature Profiles with r = 0.825 inch, Medium
       Reynolds Number, Varying UA/UF 	   51
5-43   Temperature Profiles with r = 0.825 inch, High
       Reynolds Number, Varying UA/UF 	   52
5-44   Temperature Profiles with r = 0.4 inch, Medium Reynolds
       Number, Varying UA/UF	   53
5-45   Temperature Profiles with r = 0.4 inch, High Reynolds
       Number, Varying UA/UF	   54

                                TABLES
5-1     Test Condition for Interferograms	   26
5-2    Test Conditions for Diffusion Flame With Radius of
       ftnnuTus Equal to 0.825 Inch	   39
5-3    Test Conditions for Diffusion Flame With Inner Radius
       of Annulus Equal to 0.4 Inch	   39
                                 viii

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                             ACKNOWLEDGMENTS

     Work on this contract was accomplished by personnel of the TRW Fluid
Mechanics Laboratory.  The Principal Investigator was Dr. Arvel B. Witte;
the Project Engineer, Donald E. Haflinger.  The TRW Project Manager was
Birch J. Matthews.  Technical direction and administration of the contract
for the Environmental Protection Agency was the responsibility of Mr. Wil-
liam B. Kuykendal.
        The authors wish to thank Messrs. Frank Gomes and Robert Briones of
the TRW Fluid Mechanics Laboratory for their assistance in conducting the
holography experiments.  In addition, the assistance and cooperation of Mr.
Blair Martin of the Environmental Protection Agency was greatly appreciated.
                                    ix

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                                 Metric  System Conversion  Table
SYMBOL

  in.
  ft
  yd
  Ib
  °F

  psi
WHEN YOU KNOU

 inches
 feet
 yards
 pounds
 Fahrenheit
  temperature
 pounds per
 square inch
MULTIPLY BY

  25.4
  0.3048
  0.9144
  0.453592
  5/9 (after
  subtracting 32)
  51.71
  TO FIND

millimeters
meters
meters
kilograms
Celsius
 temperature
torr
SYMBOL

  mm
  m
  m
  kg
  °C

  torr
  mm
  m
  m
  kg
  °C

  torr
 millimeters
 meters
 meters
 kilograms
 Celsius
  temperature
 torr
  0.03937
  3.28084
  1.09361
  2.20462
  9/5 (then
  add 32)
  0.01933
inches
feet
yards
pounds
Fahrenheit
 temperature
pounds per
square inch
  in.
  ft
  yd
  Ib
  °F

  psi

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                             1.   INTRODUCTION

      In  situ  probes may  be  used  to measure the properties of chemically re-
acting flows  encountered in premixed and diffusion flames.  Generally they
will  disturb  the  flow  to produce conditions not normally existent at that
point.   They  also may  require  extensive calibration of the probe to make
accurate measurements  possible.   In the current study holographic interfer-
ometry was used to "remotely sense" the index of refraction, density and
temperature fields associated  with these flames.  No flow field disturbances
were  caused in this way.
      In  order to  characterize  a  flow field uniquely, species compositicn,
two state variables, and one dynamic variable must be known.  An interfer-
ometer measurement yields the  index of refraction field, n(x,y,z).  n in
turn  is  a function of  species  mass fraction, C., and density.  In equilib-
rium, C. can  be expressed as a function of two state variables, for example,
pressure and  temperature, when the initial species fractions are known.  For
the premixed  flame in  equilibrium, the state variables and composition can
be determined uniquely for  low speed flames (constant pressure).  Data re-
duction  of the diffusion flame is likely to be more complicated because, al-
though local  equilibrium may apply, the species iray diffuse as well, leaving
the initially unreacted  composition at a point unknown.  In the present
study, techniques are  developed  using holographic interferometry to charac-
terize flame  structure and  to  obtain density and temperature profiles.  With
the current technique, averaged  measurements are made along a line of sight.
Data which exhibit axial  symmetry can be reduced to localized quantities
(radial  profiles) by means  of  inverting the integral equation for fringe
shift, a technique established by Abel and described in Reference 1.  For
the "not so axially symmetric  data" either statistical averaging techniques
have to  be used or the use  of  wide-angle holographic interferorretry and a
more sophisticated 3-D data reduction scheme must be employed.  Use of a 3-D
reduction technique was  first  applied to holographic interferorretry by
Witte2 and later  applied extensively by Matulka3.  The extent to which pro-
gress toward data reduction of these flames can be made is discussed in some
detail in this study.

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     Two burner flames were investigated.  The first, produced by an oil
fuel fired burner by Hauck, yielded far too many fringes — a condition
resulting from the fact that the burner could not be operated satisfactorily
at the low range of fuel-air rates.  The large number of fringes observed
was analogous to that measured in burners of somewhat larger size and
reported during an earlier EPA program.   This type of burner is described
in the next section; however, the flame was not studied interferometrically
because of the fringe resolution problem mentioned above.
     The second burner operated on methane and air over a wide range of
excess air and as a premixed and diffusion flame.   Holographic interferome-
tric data reduction techniques are developed for reducing the interfero-
grams recorded of this burner flame.

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                         2.   EXPERIMENTAL APPARATUS
2.1  HAUCK BURNER
     A schematic of the Hauck  Burner* is shown  in  Figure 2-1.  This  burner
has a maximum air intake  rate  of 28 cfm with a  maximum fuel intake of  1.2
gph and 0.2  gph minimum.  To operate the burner, oil  must be supplied  at ap-
proximately  20 psi to the burner pressure regulator.   Oil pressure is  reg-
ulated to  the burner from 2 to 10 psi.  A separate air blower is required
                                AIR INLET
                     OIL INLET ,
   MICRO-METERING
     OIL VALVE
 QUICK-DISCONNECT
 OIL VALVE LEVER
         A.
         B.
         C.
         D.
         E.
         F.
Single Control Lever
Inner Air Nozzle
Tangential  Inlet Openings
Oil Orifices
Stationary Outer Air Nozzle
Outer Air Nozzle Opening
        Figure 2-1.  Sectional  View of Hauck  Proportioning Oil Burner
                     and Magnified View of Nozzle  Section
   product  of Hauck Manufacturing Co., Lebanon,  Pennsylvania.

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to supply air at 0.25 psig.  The fuel oil was No. 2 distillate obtained
                                                         *
from Gulf crude.  The oil had an API gravity equal to 36.   The fuel oil
was fed to the burner from a small pressurized tank.
2.2  METHANE-AIR BURNER
     A schematic of the methane-air burner is shown in Figure 2-2.  The de-
sign concept for this laboratory methane-air burner was provided by EPA.
Additional  information was obtained from Prof A.F. Sarofim, Massachusetts
Institute of Technology.  The burner consists of two concentric cavities in-
to which the air and gaseous fuel  are introduced.  Both cavities are filled
with glass wool  to dampen feed system fluctuations and obtain uniform fuel
distribution.   The air and methane next pass through 12 gauge stainless
                                        steel tube bundle to straighten the
                                        flow and break up any large eddies.
                                        A screen separates the tube bundle
                                        and concentric cavities are housed
                                        in a 3.60-inch-diameter tube.  Gas
                                        and air are injected through a base
                                        plate.   A retainer ring and four re-
                                        tainer bolts complete the assembly.
                                        A glass chimney was initially used
                                        to preclude secondary air entrain-
                                        ment into the burner flame.  Later
                                        the glass chimney was replaced with
                                        a thinner quartz chimney for optical
                                        reasons.  To accomplish a premix
                                        flame configuration, methane is in-
                                        troduced into a 1/4-inch-diameter
                                        tube which has twenty-five 0.059-
                                        inch-diameter holes drilled in it.
                                        The tube slips inside a 1/2-inch-
                                        diameter bulkhead tee fitting carry-
                                        ing the air.  The mixer is shown in
                                        Figure 2-3.
   Figure 2-2.  Methane-Air Burner
                       \
BOTTOM PLATE
ASSEMBLY
*An API  gravity  of  36  is  equivalent  to  a  specific  gravity  of 0.845.
                                    4

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                 Figure 2-3.  Air-Methane Premix Fitting
2.3  HOLOCAMERA
     The laser holograph is comprised of a pulsed ruby laser and a holocam-
era.  The pulsed ruby is used in this investigation because sufficient en-
ergy can be produced to penetrate the burner flame during a pulse width
small enough to stop the action of the combustion phenomena.  The pulsed ru-
by laser has been described in detail in an earlier TRW report to EPA  and
will not be discussed further here.
     The holocamera design is a modified version of the greater scene depth
holocamera used in later series of tests described in Ref. (4).  The basic
modifications were as follows:
                                    1
       a)   The entire holocamera was rotated 90 degrees to permit in-
            sertion of the burner such that burning took place verti-
            cally.  To have used the.previous holocamera configuration
            would have resulted in contamination of the reference beam
            by the burner flame and resulting by-products.  The flame
            produced by vertically oriented burner is more nearly sym-
            metric than those at an angle to the gravity field.
       b)   A new finite fringe rotator to rotate the hologram verti-
            cally, was designed and built to provide horizontal fringes.

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             c)   The outer pair of lenses from the quadratic lens set,
                 referred to in Ref.  (4), was  appropriately spaced to
                 produce a focal length of 21  inches,  and apertures down
                 to 11 inches in diameter to correct for abbreviations.

             d)   Hologram and prism plate were reoriented at 52.5 degrees
                 and 75 degrees as shown on Figure 2-4 in order to reduce
                 reflections.
INCOMING
LASER
BEAM
                                        REFERENCE BEAM


                                                                          MIRROR
                                                                      •~\
                                                                        \ ^
                                                                        O^
 \   K\/
   \ I   \\ \S? 52.!
-	 i /  	^-\-
-j»M««35!
                                                                            HOLOGRAM
                                             FOCUSING
                                             LENS SET
                                                            VOLUME
                         Figure  2-4.  Schematic of Holocamera

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                             3.  TEST  PROCEDURE

      A  test  procedure was  established and followed for recording holograms
 and  interferograms  of the  burner flame.  Starting with the burner in place,
 the  following  steps were taken  to make the recordings:
        1)    Ignite  burner
        2)    Adjust  regulator pressures and flow rate
        3)    Turn  off lights
        4)    Uncover film plate
        5)    Record  the  test  scene holographically
        6)    Shut  off methane input
        7)    Record  the  comparison scene  holographically
        8)    Cover film  plate
        9)    Lights  on
      10)    Develop plate.
      Ideally,  the comparison scene  should be recorded before the test scene;
 however, with  this  burner, it was necessary to reverse the order because the
quartz  chimney had  to be removed in order to ignite the burner.  Removing
the  chimney  could leave movement fringes in the resulting interferogram.
      In the  premixed flame configuration, thermocouple readings were record-
ed during the  time  the  test  scene was holographically recorded.  Some ther-
mocouple readings were  also  taken at a later time period.  Comparison of
thermocouple readings showed that good test-to-test repeatibility could be
achieved without  any loss  in accuracy.
      In order  to  save time and  also to avoid any obscuration, wall thermo-
couple  readings for the diffusion flame configuration were also recorded at
               u
a different time  period than  the interferogram recordings.  The annulus (see
Section 2.3) was  changed to  vary the mixing region thickness as well as
overall  stoichrometry.   This modification simply requires lifting out the
center core of the  burner.
     All of the interferograms and holograms were recorded on Agfa 8E75 anti-
halation backed 4'  x 5-inch glass plates*.   Development time in Eastman Kodak
""Product of Agfa-Gevaert, Antwerp, Belgium.

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HRP developer was typically 4 minutes for an interferogram.  The acid fixer
used was Nacco fix.
     Interferograms were reconstructed with a Model 124A Spectra Physics
helium neon gas laser (X. = 0.6943|i) illuminator.  The recordings were photo-
graphed using Polaroid Type 52 film, having an ASA rating of 400.  When de-
sired, negatives of the reconstructed scene were made using Polaroid Type
55 P/N film.
                                    8

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                       4.  DATA REDUCTION PROCEDURE
4.1   INTRODUCTION
     Data reduction is comprised of three parts:  photographing the desired
view of the holographic interferogram and recording the fringe pattern using
a microdensitometer*; interpreting fringe number from the microdensitometer
trace; and computing density by means of the standard equation for fringe
shift,
                 S(x,y)    -J-   /    P(x, y, z)   p    dz             (4-1)
     The holographic interferogram is mounted in a reconstruction jig whose
orientation is the same with respect to the reference beam as it was during
the original recording of the holographic interferogram.  During reconstruc-
tion, a 15 mw continuous wave He-Ne laser (K= 0.6943 micron) was used to
illuminate the holographic interferogram.  A copy camera was positioned be-
hind the holographic interferogram.  The camera could be focused on the
event which was a known distance behind the holographic interferogram and
bounded by the viewing cone of the hologram.
     The interferograms were photographed with either Polaroid Type 55 PN
film which provides a positive and negative copy of the event using a nomi-
nal 1- to 10-second exposure at f/5.6 or Polaroid Type 52 which is about 8
times faster.  The photographic density of the fringe pattern on these neg-
atives was then recorded on a Joyce precision microdensitometer having a
slit size of about 0.010 inch by 0.010 inch.
4.2  ABEL INVERSION TECHNIQUE
     Fringe number S was measured relative to the undisturbed (light fringe)
background gas, i.e., relative to S^ = 0.  The first dark fringe occurs
where the change in optical  path isK/2.  Interpretation of the change in
optical path in wavelengths, of light, i.e., fringe number S, is aided by
keeping in mind the standard equation for fringe shift.  Starting at the
*When many fringes are available, use of the microdensitometer may be
unnecessary.

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edge of the flame the fringe number begins to decrease, the first  dark fringe
yielding a value of S   -1/2 fringe.
     The mean density profile calculations carried out here were made under
the assumption that the flow field was axi symmetric.  With the assumption
of axi symmetric flow, the equation can be inverted as the Abel integral to
obtain

                                      f*    —2 ^
                 *>"-•-*   /2   i
                                      y
                \
When this  equation is rewritten as
                              X 9  f   ds
                         "  " ^ 2      7~2
                                  J o  dr
(4-3)
it may be cast into the following finite difference form (the Schardinvan
Voorhis approximation)  for which the density is assumed constant in each of
N thin angular rings of thickness A:
                        M  1               /      o    o    /  9   9
      p(y, _ P   = -2A.  v   (s    s   )   ^k + i)2-i2- ^2-i2
       iy'    *°    TTAK  2,    k    k+1             2k + 1
                        k=T                                         (4.4)

where r.  =Ak, y = Ai and r =AN has been used and the indice  i takes on
       t\                   S
the following values:  i  =  0,  1, 2, ...,  N-l.  K is the Gladestone-Dale con-
stant, e.g., for Pffl K = 2.926 x  10"4 for air when P^ = 1 atm.

4.3  COMPARISON MODEL TO  ACCOUNT FOR SCENE DIFFERENCE
     Accounts must be made  for  different chemical species between the double
exposures creating the interferograms because the comparison scene is record-
ed with air and the test  scene  recorded with combustion products.
                                   10

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     Therefore, the Abel Inversion technique was modified to accept (3  and
 (3^ by using the Gladestone-Dale equation for a dilute gas.  The original
program was used to solve the fringe shift equation

                                                                      (4-5)

which does not account for the difference in gas composition between the
test and comparison beam recordings.  By using the Gladestone-Dale relation-
ship, n   1 = P P/PS, and the basic fringe shift equation, S = •]•• j(n-nj dz,
one gets
                        B     p    r/A   pco^   .    \
                                                     dx               (4-6)
which accounts for the difference in composition.  The Gladestone-Dale con-
stant for the reaction products of methane-air combustion, S , is shown to
             -4                                             T
be 3.208 x 10   for stoichiometric conditions.
4.4  PREMIXED FLAME FRINGE SHIFT EQUATION
     For the premixed flame configuration, further modification of the
fringe shift equation had to be carried out due to the occluded region which
appears on the edges of the quartz chimney, an observation which will be
discussed later.
     This occluded portion of the interferogram at the wall of the quartz
chimney had caused concern because initial calculation had indicated a cen-
terline temperature T/Tm  <2 for the premixed configuration, which appeared
to be far too low.  It was concluded,that the fringe shift readings within
the occluded region could not accurately be determined.  One possible method
of alleviating this source of error is to measure the waTl temperature of
the quartz chimney and to include this additional information in the fringe
shift equation.  By rearranging the fringe equation,

                         S  -  4-  /  (n   n )  dz                     (4-7)
                                           CO
                                     11

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 into two separate integrals and considering the wall temperature, then
Now, again, using the Gladestone-Dale relationship, it can be shown that the
fringe shift equation is:
- 2
    6   p
    roo  rco
                       X PC
        'COQ
                                                                      (4-9)
4.5  DIFFUSION FLAME FRINGE SHIFT EQUATION
     In the diffusion flame configuration, the same occluded region appears
on the recorded interferograms and, therefore, the fringe shift equation has
to be modified in a similar manner as presented above.   However, there is an
additional consideration that must be taken into account.  In the case of
the diffusion flame, the Gladestone-Dale constant is no longer uniform across
the chimney region and, therefore, must be varied in the evaluation of the
fringe shift equation.  In the outer portion of the chimney, there is air
with no unburned fuel nor combustion products.  Moving  towards the center of
the chimney region, combustion products are encountered, and, finally, at
the center of the quartz chimney, the gases are probably a mixture of un-
burned fuel with some combustion products.  To evaluate the fringe shift
equation, the following modification (which is shown in greater detail than
previously) must be made for the different species configuration.  The gen-
eral fringe number equation is

                           S  = 4" /  (n - n )
                                 X J

     Now, separating this equation into two separate integrals as before we
get
               S  =
  J_
   X.
njdz
/ ("» - ".
dz
(4-10)
                                     12

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    Using the Gladestone-Dale relationship, n   1   P P/PS> such that
                                  0T
                                                (species condition)
                                                (wall condition)
and
                         n   =P
                          00    CO
                                        (reference condition)
and substituting these relationships into the fringe number equation, one
gets
                                               W
                               TT
                                                         dz
                                   + 1   -
 W V + P»f W
T~ )dz + T\^	
                                                        CO
                                                  uo
                                                       '00
                                                    'dz
                                                              (4-11)
After  some algebra
_ ^^£w/&  ^^ _p .A  dz + ^/\  A  r
-  *  P.pJ     P0  pw P«    /        ^ P«\p«   / -/
                                                             dz
                                                              (4-12)
The integral /  dz can be transformed into terms of r/rQ as can be seen by
referring to Figure 4-1.
                                         1/2
                                       dr
                                                              (4-13)
                                 13

-------
                                       LIGHT RAY
                    Figure 4-1.   Diagram of  Light Beam
and therefore
   . B, i. i  M  £ Jl.  ,Vu   zS.ift   !
                                            Pco
rco
where
                                                                      1/2-
                                                                    (4-14)
               S   fringe  shift
               X = irradiation wavelength
               P = Gladestone-Date  constant
               P = density
               z = distance along light  ray
  subscripts:  ® = comparison scene condition of air burner is turned off
               T = local  test scene condition (which varies for diffusion
                   flame  configuration and is constant having combustion
                   product species  for premixed flame configuration)
               o = standard conditions at which (3's are evaluated
               w = wall  conditions
                                    14

-------
4.6  DENSITY CALCULATION PROCEDURE
     The procedure for both the premixed flame configuration and the diffu-
sion flame is about the same.  First, correct the fringe numbers by adding
the function X .    -(   - r2)     where,
                              3  P   /3   «
                     X      2 — —  I —	-
                -g-    l)  (4-15-1)   (premixed)
9  °o
   x.
                                                      (4-15-2)   (diffusion)
Now, calculate the quantity
                                                      (4-16-1)   (premixed)
                                              w
                                                      (4-16-2)   (diffusion)
Then dividing by the appropriate Y quantity one gets the density ratio,
which is the flame density normalized by the density at the conditions of
the comparison scene recording (room temperature and pressure).

     The value of  P is calculated as follows from the Gladestone-Dale equa-
tion for species i - 1, 2 ... N.  For any dilute gas,
                           n - 1
Sp.
            — J-
             poi
                                                                     (4-17)
                                        P.
                                                                     (4-18)
                                     15

-------
where P. is evaluated for species i and C- is the mass fraction.  However,
by definition
                             n - 1  = PT
                                                                     (4-19)
                                           Or
Therefore, combining these two equations yields

                                         C..P,
                                                                     (4-20)
                                    n
                                    Or
                                         roi
P -  can be shown to be 0.00279 m.  Ib_/ft  at atmospheric pressure and 0°C
where m. is the molecular weight of species i.
4.7   SAMPLE CALCULATIONS
     As an example, consider the chemical  reaction of premixed methane-air
combustion at stoichiometric conditions
            CH,
                  2"02 + 2'(3.76)N2-C02 + 2'HgO + 2'(3.76)N2       (4-21)
From this reaction, the following is calculated:
Reactions
Products
co2
H20
N2
Number of
Moles (N)
1
2
7.34
Molecular
Weight (m)
44
18
28
N x m
44
36
205.52
285.52
Mass fraction
(c,)
0.1541
0.1261
0.7198
1 .0000
Reactions
Products
C0£
N,
ci
0.1541
0.1261
0.7198
P,
4.51 x TO"4
2.54 x 10"4
2.97 x 10~4
P°i
0.12276
0.05022
0.07812
Vp0l
3.674 x TO'3
5.058 x 10"3
3.802 x 10"3
c. P
1 °i
.0189
.00633
.05623
"iV.,
5.662 x IQ'4
6.378 x TO"4*
2.737 x 10"3
                                     16

-------
 The  following  useful  parameters  can also be calculated:
      Parameter
                               Equation
                                                              Value
       CO
      1/m

      in
      p /P
       0}  
-------
     28.5
     28.0
     27.5
                    CH4 * 2 • 0+X) • (3.76) • N2

                       - CO2 + 2-H20 + 2-(HX)-(3.76)N2
              10
                     20
                            30
                                  40
                                         50
                                                60
                                                      70
                                                             80
                                                                    90
                                                                          100
            Figure 4-2.
                         AMOUNT OF EXCESS AIR, X(%)
                    Molecular Weight Versus Excess Air for
                    Methane-Air  Combustion
where X is the amount of  excess air.   Excess air is usually  defined in terms
of percent of theoretical  air.  such that:
                       AIR
                           actual
                               AIR
                                  theoretical
                                    AIR
                                                   x 100%
                                                                  (4-23)
                                       theoretical
     The amount of excess  air also affects the Gladestone-Dale  constant, p ,
for the resultant reaction product which is shown in Figure  4-3.
4.9  VELOCITY RATIO AND  REYNOLDS NUMBER
     For diffusion flames, two parameters should be defined;   (1)  the veloc-
ity ratio, and  (2) Reynolds number.
The velocity ratio is  defined as

                 U       Q   A,.
                  a      a	f  _
                                                                        (4-24)
                                        Qf *
                                     18

-------
          3.70
          3.18
          3.16
          3.14
          3.12
          3.10
          3.08
                   10
                         20
                               30
                                     40
                                           SO
                                                      70
                                                            80
                                                                  90
                                                                        100
                                  AMOUNT OF EXCESS AIR, X(°il
           Figure 4-3,
Gladestone-Dale  Constant Versus Excess Air
for Methane-Air  Combustion
where r  is  the  annulus radius, R is the  burner radius (see Figure 4-4).  Q,
                                                                            a
is the air  flow rate and Qf is the methane  flow rate.
     The Reynolds number is defined as

                                                                        (4-25)
where the density and viscosity are defined  at room temperature and pressure,
u, is the average velocity of air and methane  (u  = [uft + uf]/2), and L is
the distance  above the burner surface at which the data are being reduced.
                                     19

-------
                  t
     TTT
     AIR METHANE AIR
                            FUSED
                            . QUARTZ
                            CHIMNEY
BURNER
SURFACE
                           TUBES
                           GLASS WOOL
                          • ANNULUS
                   ANNULUS
Figure 4-4.   Methane-Air Burner
              With Annul us Insert
                20

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                               5.  RESULTS

5.1  SEQUENCE OF PROGRESS AND PROBLEMS SOLVED

     Before proceeding with a discussion of the results, a chronological
perspective of the progress and problems leading to those results  will  be
given.  The following areas were investigated and progress made as indica-
ted:

      •  Methane  burner  was  fabricated  for use  in  creating both premixed
         and diffusion flames.

      •  Finite fringe and infinite fringe interferograms were
         recorded in  diffusion  flame  configuration.

      •  Occluded region was  greatly  reduced.

      •  Laminar  premixed flame  was easy  to produce.

      t  Finite fringe interferograms were recorded of  premixed
         f1ame.

      t  Modification of data reduction procedure  to eliminate
         occluded region problem was  accomplished.

      •  Center!ine and  wall  thermocouple  temperature measurements
         were made of the premixed flame.

      •  Data reduction  of the  interferograms for  the premixed
         flame was accomplished.

      •  Finite fringe interferograms were recorded of  diffusion
         f1ame.

      •  Film fogging problem (during high flow rates in diffusion
         flame tests) solved with filters.
                                    \
      •  Wall thermocouple temperature measurements were made of  the
         diffusion flame.

      •  Data reduction  of the interferogram for diffusion flame was
         accomplished.

      •  Both laminar and turbulent flames  were observed in the dif-
         fusion flame configuration.
                                    21

-------
 5.2   HAUCK BURNER
      A small size  (as low as 0.2 gph) fuel oil-fired burner was selected for
 study because it represents a compromise between the large (1 gph) burners
 tested during a previous EPA study and the methane-air burner which is an
 approximation to the oil-fired burner for the purpose of instrumentation
 development. During testing of this burner, it was found that the flow rate,
 turbulence, and illumination were much larger than expected.  It was then
 decided that the concentration of efforts should be placed on the methane-
 air burner, because no new information could be obtained with this Hauck
 burner.
 5.3   FLAME INTERFEROMETRY
      Holographic interferograms of methane-air combustion were recorded to
 ascertain what problems might be encountered in obtaining good quality re-
 construction.  Infinite and finite fringe recordings were made both with and
 without the glass (Pyrex) chimney.  Figures 5-1 through 5-4 show the results
 of these initial interferograms of a diffusion flame.  These figures indi-
 cate  that finite fringe interferograms would be best suited for this study.
 Also, the requirement to control the ratio of fuel to oxidizer dictated the
 need  to use the chimney even though the occluded region caused additional
 problems in reducing the fringe pattern.  Note condensation in Figure 5-1.
5.4  PREMIXED METHANE-AIR FLAME
     In the premixed configuration, initial  tests were conducted under
stable flame conditions.   A stable flame is  defined as a steady blue -violet
flame which is attached at the burner surface.   It was found that when the
                         *
fuel  mixture was too rich , the flame would  rise up the chimney and go out.
In the opposite condition,  when the fuel mixture was too lean, the flame
had the tendency to be "blown" out.  Over the range of allowed operating
conditions a laminar-like flame was observed.
     Initial  holographic interferograms recorded are shown in Figures 5-5
and 5-6,  with test  conditions shown in Table 5-1.  These interferograms are
used to show the effects of the various modifications of the data reduction
procedure results.
*
 "Rich" in this case may be a misleading term since all flames were
operated with some excess air.  This burner would not operate under true
rich fuel conditions.
                                     22

-------
Figure 5-1.  Infinite Fringe Interferogram
             of Methane-Air Burner With
             Chimney
 Figure  5-2.   Finite  Fringe  Interferogram
              of Methane-Air Burner  With
              Chimney
                   23

-------
Figure 5-3.   Infinite Fringe Interferogram
             of Methane-Air Burner Without
             Chimney
 Figure 5-4.   Finite Fringe Interferogram
              of Methane-Air Burner Without
              Chimney
                    24

-------
 Figure 5-5.   Interferogram of  Pre-mixed
               Flame With Condition
               Shown in Table  5-1
Figure 5-6.  Interferogram of Pre-mixed
             Flame With Condition
             Shown in Table 5-1

                  25

-------
               Table 5-1.  Test Condition for Interferograms
Hologram
Number
5-5
5-6
Air
Regulator
Pressure
30 pslg
30 psig
Flow
Meter
16800
cc/
min
16800
cc/
min
Methane
Regulator
Pressure
30 psig
30 psig
Flow
Meter
1200 +
cc/
min
93Q
cc/
min
Conditions
S.S. screen
quartz
stack
No screen
stack on
Remarks
Air flowing
for no fire
condition
Low flame
no popping
     A comparison between Equations (4-5)  and (4-6),  as  shown in Section  4,
is made in Figure 5-7.   The solid curve is the density profile for inter-
ferogram 5-5   using Equation (4-5) for which hot and cold  combustion gases
occur in the test and comparison scenes, respectively.   The dashed curve
represents Equation (4-6) in which account is made of the change in index
between scene recordings.  The fringe shift profile used for this com-
parison is shown in Figure 5-8.   As can be seen in Figure 5-7. this first
modification tends to slightly lower the resulting density  profile as com-
pared with the original fringe shift equation.
     Note the discontinuity of the density profile at the centerline.
This discontinuity (r/r    0 of Figure 5-7) can be explained by examining
the S-curve of Figure 5-8.  The maximum in the S-curve is to the left of
center, such that ds/dr   ,   _ Q * 0.  The inverted fringe  shift equation
for density                °
                    p(y)  B
                             i  -
                      00
                                  TTKD
                                     CO
i:
  dr£
(r2 - y2)
                                                      V2
shows that with a negative ds/drl.   _ n the density will  be initially
                                 r/rQ - u
larger than if the ds/dr^r  _ Q is positive.  Thus, the density is dis-
continuous as r approaches r = 0, a condition which is physically impossible
   Interferograms will be identified by their figure number.
                                    26

-------
                              P
                             _P_

                              Poo
Figure 5-7.  Comparison Between Equations  (4-5)  and  (4-6)  for
             Interferogram Data EPA  No.  5-5

-------
                                     r
                                     ro
           Figure 5-8.  Fringe Shift for Interferogram No. 5-5

for this flow problem.  Figure 5-9 shows a similar phenomenon for inter-
ferogram 5-6.  In this figure, the solid curves indicate the computed
density across the quartz chimney with the same discontinuity shown at
r/rQ = 0.  For axisymmetric flow, ds/dr is zero.  Therefore, to eliminate
the density discontinuity, the left and right sides of the S-curve were
averaged.  The dashed curve in Figure 5-9 is the result of S-curve aver-
aging. Figure 5-10 shows the actual fringe shift and the average fringe shift
for interferogram 5-6.
     The temperature ratio T /T is just the inverse density ratio P/p
                            co                                       reo
since the molecular weights are nearly the same.  The centerline tempera-
ture ratios for these two interferograms appear far too low, T/T^ 2.  This
problem was discussed earlier in Section 4 and will be given further
treatment later on in this section.
     For the density calculations up to this point it was assumed that
stoichiometric conditions exist.  (See Section 4.8 and Figures 4-1 and
4-2).  To show what effect the amount of excess air has on the calculation
                                     28

-------
ro
                             AVERAGED
                             SOLUTION
        1.0
.6
.4
.2
0

r
.2
.4
.6
.8
1.0
                          Figure 5-9.   Density Solution for Interferogram EPA No.  5-6

-------
                                    —2
     1.0   .8
.6
.4
.2
.2    .4
.6
..8
          Figure 5-10.   Fringe Shift for Interferogram EPA No.  5-6

of the density profile, a sample case was done using interferogram 5-6,
The results are shown in Figure 5-11.  The solid curve is the density
profile as defined by stoichiometric conditions.  The dashed curve is the
density profile with an assumed 100 percent excess air (twice the amount
of air needed for stoichiometric conditions).   Allowing for the amount
of excess air will lower the density for any one fringe shift profile.
     In Figures 5-1 and 5-2, about 50 percent scene within the Pyrex
chimney region is occuluded and, therefore, it is impossible to make any
determinable conclusion about the fringe shift profile in the occluded
portion of the chimney.  The Pyrex chimney has a wall thickness of 2.5
millimeter.  By replacing this chimney with a fused quartz chimney with
a wall thickness of 1.5 millimeter, the occluded regions were sufficiently
decreased even though some waviness in the wall is observed.  The result of
this change decreased the occlusion to about 10 to 20 percent.
     Since the quartz chimney also produced some occlusion, it was decided
to use a rectangular box with Pyrex windows, used on an earlier EPA pro-
gram, to circumvent the occluded areas produced by the edge of the round
quartz chimney.  An adapter was designed and fabricated to permit the
                                    30

-------
    1.0
                                        STOICHIOMETRIC CONDITIONS
                                        100% EXCESS AIR CONDITIONS
P_
P.
           Figure 5-11.   Effect of Excess Air on Density Profiles for Interferogram No.  5-6

-------
mounting of the glass sealed box around the methane-air burner.  Figure
5-12 shows an interferogram recorded with this configuration.  The chief
problem encountered with this approach is that the flame has a tendency
to "wander" about inside the box, a characteristic which is not conducive in
providing axisymmetric phenomona.  For this reason, the rectangular box
approach was abandoned.
     It was noted earlier that data reduction procedures up to this point
produce center!ine temperatures which were too low.  Referring to the
modification in  Section  4.4, a sample calculation was made using the data
recorded in interferogram 5-6 to illustrate the feasibility of this
                                                                  *
procedure.  It was assumed that the wall  temperature was T /T^ = 2  and
that stoichiometric combustion occurred.
     A comparison between previous methods and this approach is shown in
Figure 5-13.  The centerline temperature is now calculated to be
which is in a more probable temperature range.
            Figure  5-12.  Test  Interferogram for Rectangular Box
                         with  Pyrex Windows
*
 Thermocouple data support this value.
                                      32

-------
oo
Co
                 .8 -
           P

           pob
                 .6
                 .5
                 .4
                  .3
                 .2
                                                                                                  CD
                                                                                               CD
                            .1       .2       .3       .4
.5       .6
.8
.9      1.0
                 Figure 5-13.  Effect of  Wall  Temperature on  Density Profile for  Interferogram No. 5-6

-------
     To apply the data reduction method above, chimney wall and gas center-
line thermocouples were installed.  The two wall thermocouples were of
copper-constantan type.  The thermocouples were bonded with sauereisen
to each side of the fused quartz chimney at the scene centerline.  The
wall temperature was measured to be 456°F.  The fused quartz chimney
centerline thermocouple was of a chromel-alumel type.  The gas centerline
temperature was measured to be 1670°F.  The air and methane were measured
as 49870 cc/min and 4578 cc/min, respectively.
     Two interferograms were taken at the same test conditions as were
reported above.  Also, additional thermocouple readings were recorded to
insure repeatability of the initial test.  These readings were well within
1  percent of the original readings.  Figure 5-14 shows one of the inter-
ferograms recorded and used for data reduction purposes.  All three thermo-
couples can be seen in this interferogram.
     In order to validate the temperature calculated by the fringe shift
recorded on the interferograms, comparisons were made to the gas temperature
readings that were recorded from the thermocouple measurements and those
computed from a theoretical adiabatic flame temperature calculation for
a premixed methane-air flame.  The method used included the dissociation
of the combustion products over a range in percentage of excess air.  This
            Figure 5-14.  Interferogram with Thermocouples Attached
                                     34

-------
method is described in a book entitled "Flames" by A. 6. Gaydon and H.  G.
Wolfhard.  The results of this computer program are shown in Figures 5-15
and 5-16.  In Figure 5-15, the temperature decreases as the percentage
of excess air is increased from stoichiometric conditions (zero percent
excess air) to 300 percent excess air.  In Figure 5-16, the various com-
bustion products are shown in terms of their individual partial pressures
and how they are related to the percentage of excess air.  Both the tempera-
ture and partial pressure of the combustion products have been verified
at stoichiometric conditions.   In Figure 5-17, the density profile for
interferogram 5-14 is shown.  The results of the measured fringe shift
from this interferogram indicates a centerline temperature of 1777°F, which
is much lower than the theoretical temperature at the indicated value of
14 percent excess air for this case.  However, the fringe shift calculation
of temperature is higher by 6 percent than the recorded thermocouple read-
ings which are expected to be low because neither radiation nor heat con-
dition.loss corrections were made.  The differences between the theoretical
temperature and those of the fringe shift calculations and the thermocouple
temperature reading may be caused by heat loss to the surroundings since
the measurements were taken 3 inches above the actual burning surfaces.
5.5  DIFFUSION METHANE-AIR FLAME
     Since a turbulent flame could not be produced in the premixed con-
figuration, diffusion flames were studied to:  (1) discover if a turbulent
flame could be produced and a data reduction scheme provided for it, and
(2) determine what effect, if any, fuel injection radius and air annulus
radii would have on the temperature profiles.
                                     i
     In the study of effect of annulus radius, two annuli of different
radii were used.  The choice of annulus radii was somewhat arbitrary.
However, to make a comparison of the effect that the annulus radius has on
temperature profiles a significant difference in radius should be used.
Thus, the inner annulus radii were selected to be 0.825 and 0.4 inch.
Interferograms were taken at five different velocity ratios obtained by
varying the amount of excess air at a given fuel  rate.  The range of excess
air provided by the larger annulus radius is from 0 to 300 percent.  Also,
it was attempted to vary the Reynolds number by two orders of magnitude.
                                    35

-------
                       3000
                    T<«F)
                        2000
Ok
                        1000
                                                  100
                                        200
300
                                                         %EXCESS AIR
                   Figure 5-15.
Temperature of Methane Air Premixed Flame Versus Percent  Excess Air
Assumed:  Dissociation of combustion products and no  losses  due to
radiation, conduction nor convection)

-------
       50         100         150         200
                Percent of Excess Air
250
300
Figure 5-16.   Partial  Pressures  of  Combustion Products
                          37

-------
Then, using the smaller annul us, a comparison series of tests was conducted.
The flow rates for this series of tests were taken such that the velocity
ratios remained the same, and the velocities of the individual gases were
also the same between the two test series.  However, the range of excess
air was altered as dictated by the velocity requirements stated above.
     In order to maintain the same velocities between these series of
tests, the volumetric flow rates for each gas were adjusted according to
the following:
where subscripts 1 and 2 refer to test series 1 and 2, respectively, and
where Q is the flow rate and A is the area.  By expressing this relation-
ship in terms of the respective radii, one obtains for each gas,

                                 n(R2 - r 2)
                       Q2  -  Q,—5	2  (A1r)
                        2      ] rr(R2   r/)
and
                                             '(Methane)
Therefore, when using the smaller inner radius (r« = 0.4) for the second
test series, the air flow rate was increased by a factor of 1.39, and the
methane flow rate was decreased by a factor of 4.25.  This considerably
increased the range of excess air from 489 to 2260 percent for the second
series of tests.  The test conditions are shown in Tables 5-2 and 5-3.
These tables also include wall thermocouple temperature results and some
visual flame descriptions.
                                     38

-------
  Table 5-2.  Test Conditions for Diffusion Flame with Radius
              of Annul us Equal to 0.825 Inch
Reynolds No.
Factor




1




2




3

*,*
•; Excess
fir

0
50

100
ZO'J
300
0
50
100
200
300
0
50
100
200
300
Flow Rate (cc/min)

Air
945
1,120

1.8JO
2,340
3,780
9,450
14,200
18,900
28,400
37,800
04,500
142,900
189.JOO
284 ,000
373,000

1 'ethane



99.1




991.0




9910.0


Velocity
Patio
u la.
a T
3.15
4.72

G.29
9.45
12.58
3.15
4.72
6.29
9.45
12.58
3.15
4.72
6.29
9.45
12.53
He
T






158
483
662
G45
1,210
1 ,580
1,330
6.S20
0,450
12, ua
15,800
Ti
T Very turbulent flame
                              39

-------
      .6
      .5
     .4
-p-   .3
 roo
      .2
                           .2
           .4       .5
.6
.7
.8
.9       1.0
                     Figure  5-17.
Density Profile for Interferogram No.  5-14 With
14 Percent Excess Air

-------
     For the interferogram data reduction procedure of the diffusion flame,
the chimney cross section was divided into three regions (as shown in
Figure 5-18):
     1)   The outer most region of the annulus was considered pure air.
     2)   The next region (moving towards the centerline) was identified
          as the stoichiometric combustion zone.
     3)   The centerline region was considered as pure unburned methane.
     Using this description of zones in initial evaluation of temperature
(results not shown), it was found that when the third region was assumed
to be pure methane, very low temperatures at the centerline were computed
(T/Tg, < 1).  Also, the temperature profile would markedly differ in the
third region if the thickness of this region was varied.  To explain
further, the temperature would "drop" as the temperature profile passed
through the second region to the third and, therefore, showed a dependency
           L '
on the selected location of the boundary between these regions.  This
problem does not occur between the first and second region and was tested
by shifting the location of their boundary.
     Since the location of the third region boundary greatly influenced
the temperature in the third region, it was not possible to define this
region clearly.  However, the location of the third region does not affect
the calculation of the peak temperature in the temperature profile because
the composition at the peak temperature is dominated by air and combustion
products whose index and Gladestone-Dale relationships do not differ
significantly.  This problem cannot be solved using interferometry alone,
but requires a separate measurement of gas composition.
     Figures 5-19 through 5-29 are interferograms of the diffusion flame
with r = 0.825 inch and with excess air, x, and velocity ratio, ug/uf as
shown.  The peak temperature, taken from the reduced temperature profile
                                     47

-------
                                         TYPICAL
                                          FRINGE
                                          PATTERN
Figure 5-18.
Schematic of Typical  Fringe Pattern Divided
Into Its Three Compositional  Regions
                       Figure 5-19

                       r  = 0.825

                       u  = 0.0267

                       ^ = 12.58

                       x  = 300%

                       I  = 3.13
        Figure 5-19.  Reconstructed Interferegram

-------
00
                                        Figure 5-21
r =
U =
i i ~
uf
x =
I =
0.825
0.0817
3.15
0%
2.89
r =
u =
	 =
«*f
X =

0.825
0.112
4.72
50%
4.0
Figure 5-22
r   =  0.825
u   =  0.143
$  =  6.29
x   =  100%
I-   =  3.03
Figure
r =
u
"a _
uf
x =
I =
5-23
0.825
0.205
9.45
200%
3.3
Figure
r =
u =
uf
x =
I =
5-24
0.825
0.267
12.58
300%
4.0
                                 Figures 5-20 through  5-24.   Reconstructed Interferograms

-------
Figure
r =
U =
ill =
uf
x =
I-
5-25
0.825
0.817
3.15
0%
4.30
Figure
r =
u =
"a _
uf
x =
t =
5-26
0.825
0.817
4.72
50%
3.65
Figure
r =
u =
ua _
uf
x =
1 =
T.O
5-27
0.825
1.12
6.29
100%
3.97
                                                       Figure 5-28

                                                       r  =  0.825
                                                       u
                                                          =  1.43
                                                          =  9.45
                                                       "f
                                                       x  =  200*

                                                       I  =  3.0
Figure 5-29
r  =  0.825

u  =  2.05

^ -  12.58
"f
x  =  300%

      4.41
1   =
Figures 5-25  through  5-29.   Reconstructed  Interferograms

-------
data, is also shown in the legend of each figure and is plotted later on.
The sequence of photographs are in order of increasing Reynolds number.
Fringe shift near the wall is minimal, indicating small changes in tempera-
ture.  Proceeding inward towards the center!ine, the abrupt fringe shift
results from the lower density, higher temperature "flame sheet" occurring
at the air-fuel interface.  The trend with increasing Reynolds number which
is directly proportional to
is that the flame width decreases, a result consistent with a laminar mixing-
reaction zone.  The interferometric data for r = 0.4 inch are shown in
Figures 5-30 through 5-39 and exhibit the same trends as the data at
r = 0.825 inch.
     During some preliminary work conducted before actual interferometry on
diffusion flames, thermocouple measurements were taken.  The thermocouple
was located about 0.25 inch above the burner surface and emersed at the edge
of the visible flame front.  This location was selected after some probing
was done to find where the maximum temperature occurs.  (It should be noted
that when reducing the interferogram data, it was not always possible to
select a fringe which corresponds to the thermocouple location.)  The
results of the thermocouple measurements indicate only a slight increase in
temperature with increase of excess air.  The phenomenon differs greatly
with the findings of premixed flame configuration which indicated a sub-
stantial temperature dependence on the percentage of excess air.
                                     45

-------
CTl
Figure 5-30
r   =  0.4
u   =  0.0817
Hi  =  3.15
uf
x   =  489%
                  T
                  T_
5.5
Figure 5-31
r   =  0.4
u   =  0.112
Hi  =  4.72
uf
x   =  786%
I   =  3.95
Figure  5-32
r   =   0.4
U   =   0.143
Hi  =   6.29
uf
x   =   1080%
T   =   4.17
                                                                                                 Figure 5-33
                                                                                                 r  =  0.4
                                                                        0   =  0.205
                                                                        Hi
                                                                        uf
                                                                            =  3.33
                                                                                                 Hi =  9.45
                                                                                                 x  =  1680%
                                                                                                 T
Figure  5-34
r   =   0.4
u   =   0.267
Hi  =   12.58
x   =   2260%
I   -   3.33
                                     Figures  5-30  through 5-34.   Reconstructed  Interferograms

-------
Figure 5-35
r   =  0.4
u   =  0.817
Si-  -  3 IS
uf    J>lt>
=  489%
=  3.16
                      Figure 5-36
                      r   =  0.4
                            1.12
                            4.72
u
Hi
uf
x   =  786%
                      ±   =2.30
                          Figure 5-37
r   =  0.4
u   =  1.43
Sf  •  «•»
x   =  1080%
      2.40
                          Figure 5-38
                          1   =
                          L
r
U
"f
x
T
TL
0.4
2.05
9.45
1680%
3.10
Figure
r =
u =
uf
x =
1
t
5-39
0.4
2.67
12.58
2260%
4.68
               Figures 5-35  through 5-39.   Reconstructed Interferograms

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     Figure 5-40 shows the peak temperature as a function of averaged
streams' velocities,"!?, which provides a Reynolds number per unit length range
of two orders of magnitude, varying from~160 to 16,000 per foot.   The mean
temperature appears to be about I/Ten ~ 3.5 or T = 300 x 3.5 = 1050°K
(1430°F).  Disallowing the one high data point near "u" = 0.08 ft/sec, vari-
ations of the data about the mean temperature increase with u or Re.  This
observation is consistent with the idea of an unstable laminar flame sheet
in the transition region.  Recall that at the highest Reynolds numbers the
flame looks turbulent.  See especially the highest Reynolds number interfero-
gram data at r   0.4.
     The solid curve in the intermediate range of IT represents flame thermo-
couple measurements.  Good agreement is obtained with the interferometric
data.  No corrections  were made to the thermocouple measurements for
radiation losses.  By  using the radiation correction model developed on the
earlier EPA contract,  a correction to increase the measured temperature by
about 20 percent is indicated.  This correction would place the measurements
very near the upper range of the interferometric data rather than at the
average.
     Local  temperature profile data are shown in Figures 5-41, 5-42 and
5-43 at r = 0.825 inch and Figures 5-44 and 5-45 at r = 0.4 inch.   Shown in
the legend are also the values of excess air, x, velocity ratio u,/u^, and
                  	                                             or
average velocity, u.  Examination of these data reveal the following
trends:
     a)    Strong TT  (Reynolds number) dependence on the peak tempera-
          ture location is observed for constant ua/uf and x for a
          102 range in Reynolds number.  As Re increases, the flame
          sheet moves  towards the air side.  This result is Indicative
          of what might be expected of a turbulent flame or a
          "transitional" flame (Figure 5-41).
     b)    For each r value of the annulus (compare Figures 5-42 and
          5-43 and  5-44 and 5-45), this same effect is observed inde-
          pendent of velocity ratio of excess air.
                                     48

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     6 r
                                        D
      5 ~
     oo
                                                 D
                                                           o
                                                                            o
                                           o
                                                                                 o
                                                                                               D
                                                                                               o
                                                                                           8
vo
                        O   r = 0.825

                        D   r = 0.4

                            THERMOCOUPLE DATA
       10
         -2
10
  -1
J( FT/SEC
                         Figure 5-40.  Plot of Peak Temperatures of Reduced  Interferograms
                                       and Thermocouple Data

-------
                                                              X   UA/UF    U
                                                           1  300   12.58   .0267
                                                           2  300   12.58   .267
                                                           3  300   12.58   2.67

Figure 5-41.  Temperature Profiles With  r = 0.825 inch, Varying Reynolds Number,
              Constant UA/UF

-------
K.O
O.I'...
1.2      0.3
RxRCO)
0.
0.5
0.6
0.7
0.8
                                                 0.9
                                                 1*0
         Figure 5-42.  Temperature  Profiles  With r = 0.825 inch, Medium Reynolds Number,
                       Varying UA/UF

-------
ro
                                                                                                     X   UVUF   U
                                                                                                     0   3.15    0.825 B
                                                                                                         4.72    1.12
                                                                                                                 1.43
                                                                                                                 2.05
                                                                                   2  50
                                                                                   3  100  6.29
                                                                                   4  200  9.45
                                                                                   5  300 12.58
IllJi!!  ii
:» ,::  .:  :.  : :!••:.::;:;:::::::::::::::::::::::::::::::::::;::::::
   <'   :   i:  : r:;\: "::::::::: :i
   IX   i      i _.- ..i.. ,.•••    .  ,
   *«   "   • 5  • «•!*"••!•••••••••••••  •          :    ...   . •
   ."   •   " -  t -  «••••••••!•••••••••••••••!•••••••••••••••••••!•••••••
   •          " •••••••••••••••••••••••••••••••••••••••••••••••!••••••«
   •    •   • •  I •I•••••«••••••••••••••••••••••••••P«*••••!•••••••••••••
   •    I   • •  • •••••••••••••••••••••••••••••••••••••••••••••••!•••••••
   :    :   ::  : i:::::::::::::::::::::::::::::::::::::::::::::::::
   :    :   : :  : ::::::::::::::::::::::::::::::::i:::::::::::::::::::::::
                                                                                            	

              0.0       O.J
0.2        0.3        Q.*         0.5
 RsRlO)
                                                                                     = 0.825 INCH
                                                                        0.6
                          Figure 5-43.   Temperature  Profiles With  r =  0.825  inch,  High  Reynolds  Number
                                            Varying UA/UF

-------
U1
CO
                                                                               X   U/VUF
                                                                          | 1. 489   3.15    .0817
                                                                          •2. 786   4.72    .112
                                                                           3.1080   6.29    .143
                                                                          ]4. 1680   9.45    .205
                                                                          J5. 2260  12.58    .267
                                          r=0.4 INCH
                                0.2       0.3
                                RxFUO)
0.5
0.6
0.7
o.a
0.9
                                                    1.0
                      Figure 5-44.  Temperature Profiles With  r
                                     Varying UA/UF
     = 0.4  inch, Medium  Reynolds Number,

-------
01
-pi
                                                                              X   UA/UF   U
                                                                          1   489  3.15    .817
                                                                          2   786  4.72    1.12
                                                                          3   1080  6.29
                                                                          4   1690  9.45
                                                                          5   2260 12.58
:o.o     o.i
                                                                                              0.8
0.9
1.0
                       Figure 5-45.   Temperature Profiles With  r = 0.4 inch,  High Reynolds Number,
                                      Varying UA/UF

-------
c)   For a given Re, considerable variation in position of peak
     temperature signal is present.  This is believed to be
     caused by the fluctuating or transitional character of the
     flame zone.

d)   No clear difference exists between the r = 0.4 and 0.825 inch
     cases.
                                 55

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                    6.  CONCLUSIONS AND RECOMMENDATIONS


6.1  CONCLUSIONS

6.1.1  Interferometrlc Data Reduction Procedures

     a)   The basic equation for fringe shift was  inverted  to provide
          unique determination of the density field for the case of
          axisymmetric phenomena, which turned out to be a  fairly
          good approximation in most cases.   Modifications  were
          included for differences in molecular weight and  refractive
          index between the reference and  test scenes of the burner.

     b)   A data reduction model  was developed which allowed the
          reduction of interferometric data  when the chimney wall
          became hot.   Basically, the procedure allowed the incorpora-
          tion of a thermocouple wall temperature  measurement which
          obviated the high fringe density and internal reflection
          present at the chimney wall for  the premixed flame.

     c)   It was shown by calculation that errors  in knowledge of the
          composition  for the premixed flame produced small errors in
          the final computed density and temperature field  because
          the index, index-density, and density-temperature relation-
          ships were dominated by those properties of air,  at least
          for those conditions investigated  here for stoichiometric
          and excess air combustion.

     d)   For the data reduction model developed for the diffusion
          flame, it was found that the air side of the flame could
          be computed somewhat independently of knowing what the
          actual species composition was in  the diffusion layer
          whereas the features of the fuel side of the sheet were
          strongly dependent on the composition in the diffusion
          layer between the fuel  and the flame sheet.  Thus, the
          overall variation of index, index-density, and density-
          temperature across the flame is  too large to expect an
          interferometric measurement alone  to provide temperature,
          at least for the fuel side of the  flame  sheet.

6.1.2  Diffusion Flame

     a)   The diffusion flame was operated over a  Reynolds number
          range ojMOO.  Reynolds number per unit  length,
          Re/L = u/y,  was varied by increasing both air and fuel flow
          rates and by increasing the air  flow rate (increasing
          percent excess air) at fixed fuel  rate.

     b)   Variations about the peak temperatures calculated from
          these data increased as a function of Reynolds number.
          This phenomenon is believed to be caused by the  increas-
          ing frequency of unstable spots  (turbulent spots)  in the
          flame sheet.

                                     56

-------
     c)   Thermocouple data  provided excellent agreement with mean
         of  the  interferometric data.

     d)   The large  range  in Reynolds  number  investigated provided
         data for the diffusion (laminar) flame and at the highest
         two Reynolds number,  data for  the turbulent flame.

6-1.3  Premixed  Flame

     Largely  because of the extensive work done to provide a suitable data

reduction procedure for the case of the premixed flame, i.e., to account for

the occluded  region at the chimney wall, data were recorded and reduced at
only one Reynolds number and one value of excess air.   Good agreement was

obtained between the thermocouple inserted in the flame and the interfero-

metric data albeit the measurements were much lower than the adiabatic flame
temperature.

6.1.4  Oil  Burners
     At present, holographic interferometry does not appear applicable to

highly turbulent-complex-real flames (i.e., oil burners).  However, labora-

tory flames that are in the transitional or slightly turbulent regime can
be evaluated by this technique.

6.2  RECOMMENDATIONS

     a)   Future studies should be conducted with a wrap-around
          180-degree viewing-angle holographic interferometer to
          provide adequate three-dimensional coverage so as to allow
          accurate measurement of strongly asymmetric flames caused
          by either or both turbulence or asymmetric burner
          configurations.

     b)   Diffusion flame cannot be analyzed quantitatively by
          interferometry alone.  A mass composition probe is neces-
          sary to provide data on the fuel-side diffusion zone of
          the flame sheet.  It does not appear that a complicated
          non-equilibrium sampling procedure is justified since the
          index of the non-equilibrium products properly averaged
          may be equal to the equilibrium value.  Thus, a simple
          aspirating probe may be adequate.

     c)   It is strongly recommended that the feasibility of chemi-
          luminescent spectroscopy be examined to measure local
          chemical  species concentrations as well as temperature
          profiles  in flames of this type.  This technique has re-
          cently been developed and used successfully on several
          chemical  laser programs at TRW.  Its chief advantage lies
          in being  able to make the measurement remotely without
          disturbing the flow.
                                    57

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                               REFERENCES
1.  F. 0. Weyl, "Analytical  Methods  in Optical  Examination  of  Supersonic
    Flow," Navord Report 211-45,  Navy Department Bureau  of  Ordnance,
    Washington, D.C., 11 December 1945.

2.  A. B. Witte, "Three Dimensional  Flow Field  Analysis  by  a Holographic
    Interferometry," Final Technical  Report,  TRW Report  No. 12414-6005-RO-OO,
    15 February 1971.

3.  R. D. Matulka and D. J.  Collins,  "Determination  of Three-Dimensional
    Density Fields from Holographic  Interferograms,"  Journal of Applied
    Physics, 42, 1109, March 1971.

4.  A. B. Witte and B. J. Matthews,  "Laser Holography Study of Oil-Fired
    Burner Combustion," EPA  Contract  CPA 70-4,  TRW Report No.  14103-604-RO-OO.

5.  A. G. Gaydon and H. G. Wolfhard,   Flames. Their  Structure, Radiation
    and Temperature, 3rd edition, Chapman and Hall Ltd., London,  pp.  288-304,
    1970.

6.  R. Friedman and J. B. Levy, Combustion and  Flames. 7, 195, 1963.
                                   58

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                                TECHNICAL REPORT DATA
                          (Please read Instructions on the reverse before completing)
 \, REPORT NO.
 \,        . .
 EPA-650/2-74-031-a
                                                      3. RECIPIENT'S ACCESSION>NO.
4. TITLE AND SUBTITLE
Application of Holographic Methods to the Measurement
  of Flames and Particulate, Volume I
                                  5. REPORT DATE
                                   April 1974
                                  6. PERFORMING ORGANIZATION CODE
                                                        11982
7. AUTHOH(S)
A..B. WitteandD.E. Haflinger
                                  8. PERFORMING ORGANIZATION REPORT NO.

                                    23523-6001-TU-OO
9. PERFORMING OROANIZATION NAME AND ADDRESS
TRW Systems Group
One Space Park
Redondo Beach, CA  90278
                                  10. PROGRAM ELEMENT NO.
                                   1AB014; ROAP 21ADG-51
                                  11. CONTRACT/GRANT NO.
                                   68-02-0603
12. SPONSORING AGENCY NAME AND ADDRESS

SPA, Office of Research and Development
NERC-RTP, Control Systems Laboratory
Research Triangle Park, NC 27711
                                  13. TYPE OF REPORT AND PERIOD COVERED
                                   Final
                                  14. SPONSORING AGENCY CODE
IS. SUPPLEMENTARY NOTES
16. ABSTRACT
          The report gives results of the application of a pulsed ruby laser holo-
graphic interferometer to the study of flames, in hopes of extracting temperature
jrofile data. The principle  involved is to record holographically the interferogram
which presents a three-dimensional record of the interference fringe pattern. The
density profile and hence the temperature profile can be calculated from the fringe
shift information. The report presents data for a methane-air burner operating both
as a diffusion flame and as  a premised flame. The large number of fringe shifts
recorded on an interferogram complicated the reduction of the methane-air data, but
it was possible to correlate the interferometrically derived temperature data with
thermocouple measurements. Application of the technique to a 0.2 gal. /hr oil burner
was unsuccessful because the highly turbulent flame caused an interference pattern
:hat could not be deciphered.
                             KEY WORDS AND DOCUMENT ANALYSIS
                DESCRIPTORS
                                          b.lDENTIFIERS/OPEN ENDED TERMS  C.  COSATI Field/Group
    Pollution
 holography
 interferometers
 Femperature Measurement
 jlame Photometry
 Combustion
Diffusion Flames
Air Pollution Control
Holographic Ihterfero-
            metry
Flame Measurement
Combustion Research
Premised Flames
13B
14B
20F
                                              21B
 9.-DISTRIBUTION STATEMENT
                      19. SECURITY CLASS (Tliis Report)
                      Unclassified
                                                                   21. NO. OF PAGES
                                                                   69
Unlimited
                      20. SECURITY CLASS (Tills page)
                      Unclassified
EPA Form 2220-1 (9-73)
                                         59

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