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      The ENVIRONMENTAL, HEALTH SERIES of reports was
established to report the results of scientific and engineering
studies of man's environment:  The community,  whether urban,
suburban,  or rural, where he lives, works, and plays; the air,
water, and earth he uses and re-uses; and the wastes he pro-
duces and must dispose  of in a way that preserves these natural
resources.  This SERIES of reports provides for professional
users a central source of information on the intramural research
activities of Divisions and Centers within the Public Health Ser-
vice, and on their cooperative activities  with State and local agen-
cies, research institutions, and industrial organizations.  The
general subject area of each report is  indicated by the two letters
that appear on the publication number; the indicators are

                   AP - Air Pollution

                   AH - Arctic Health

                   EE - Environmental Engineering
                   FP - Food Protection
                   OH - Occupational Health

                   RH - Radiological Health
                   WP - Water  Supply  and Pollution Control

      Triplicate tear-out abstract cards  are provided with re-
ports in the SERIES to facilitate information retrieval.  Space is
provided on the  cards for the user's accession number and addi-
tional key words.

      Reports in the SERIES will be distributed to requesters, as
supplies permit.  Requests should be directed to the Division
identified on the title page or to the Publication Office, Robert A.
Taft Sanitary Engineering Center, Cincinnati, Ohio 45226.
  Public  Health Service Publication No.  999-AP-24

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                       CONTENTS
    ABSTRACT	    v
 I. INTRODUCTION	    1
 II. SUMMARY OF EMISSION DATA	    3
III. PROPERTIES AND DISTRIBUTION OF COAL  ....    7
        Introduction	    7
        Coal Production and Distribution	    7
        Chemical Properties of Coal	    9
             Classification of Coal	    9
             Typical Properties of Coal by Producing
                Districts	    11
             Coal Ash	    12
             Sulfur in Coal	    14
             Chlorine in Coal	    14
        Physical Properties of Coal	    19
             Coal Sizing	    19
             Fusibility of Coal Ash	    19
             Coking and Caking Properties of Coal ....    21
IV. COAL COMBUSTION THEORY	    23
        Combustion  of Coal	    23
        Combustion  in Fuel Beds	    25
        Combustion  of Coals in Suspension	    28
 V. HOW COAL IS UTILIZED	    31
        Brief History of Development of Mechanical
           Firing Methods	    31
        Description  and Size Ranges of Mechanical
           Firing Equipment	    32
             Underfeed Stokers, Single-Retort,
                Residential	    32
             Underfeed Stokers, Commercial, Institu-
                tional,  and Small Industrial	    32
             Multiple-Retort Underfeed Stokers	    33
             Traveling-Grate and Chain-Grate Stokers  .  .    33
             Vibrating-Grate Stoker	    35
             BCR Automatic "Packaged"  Boiler	    35
             Spreader Stoker	    36
             Pulverized-Fuel Firing Units	    37
             Cyclone Furnace	    38
        Summary of Related Coal-Firing Equipment
           and Use	    39
VI. SMOKE EMISSIONS AND COMBUSTION PLUME ...    41
        Theoretical  Considerations	    41
                             111

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          Plume Emission Measurement Methods	    42
              Ringelmann Chart	    42
              Equivalent Opacity	    42
              Soiling Potential	    42
              Smoke Spot Tester	    43
          Plume Emission Data	    43
              Smoke in Average Percent Density	    43
              Plume Equivalent Opacity	    44
              Soiling Potential	    45
              Smoke Spot Data	    45
              Mass Emission and Smoke Plume	    46
          Reducing Smoke  Emissions	    48
              Hand Firing	    49
              Small  Underfeed Stokers	    49
              Large Boiler-Firing Equipment	    49
 VII.  PARTICULATE EMISSIONS	    51
          Theoretical Considerations	    51
          Emission Units	    53
          Physical Properties of Particulates	    54
              Particle Size Distribution	    54
              Particle Description	    58
              Particle Density	    59
          Chemical Composition of Particulates	    60
          Combustible Content of Particulates	    63
          Mass Emission  Factors	    65
              Effect of Firing Rates on Emissions	    73
              Hand-Fired  Units	    74
          Control of  Particulate Emissions	    76
          Variables Affecting Efficiency of Control
             Equipment	    79
VIII.  GASEOUS EMISSIONS FROM COAL COMBUSTION .  .    83
          Sulfur Oxides	    83
              Theoretical Considerations	    83
              Emission Data	    83
          Oxides of Nitrogen	    87
              Theoretical Considerations	    87
              Emission Data	    89
          Other Gaseous Emissions	    91
 IX.  FUTURE NEEDS FOR DATA AND RESEARCH  ....    93
          Emission Data Needs	    93
          Research Needs	    93
          Suggested Research Directions	    95
      REFERENCES	  .    97
      ACKNOWLEDGMENT	!.  .   Ill
                             IV

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                        ABSTRACT
      Information concerning atmospheric  emissions arising
from the combustion of coal was collected  from the published
literature and other sources.  The data were abstracted,
assembled,  and converted to common units of expression to
facilitate comparison and understanding.  From these data,
emission factors were established that can be applied to coal
combustion processes  to determine the magnitude of air pollu-
tant emissions.  Also discussed are the composition of coal,
theory of coal combustion, emission rates, gaps in emission
data,  and future research needs.

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           ATMOSPHERIC  EMISSIONS
          FROM COAL  COMBUSTION  -
             AN  INVENTORY GUIDE
                       CHAPTER  I.
                   INTRODUCTION
      Although smoke, liquid and solid particles, and gases
 from the combustion of coal have long been an almost universal
 contributor to air pollution, information published on the subject
 has been largely fragmentary.  For this reason the Technical
 Assistance Branch  of the Division of Air Pollution undertook a
 project to draw together existing knowledge concerning emis-
 sions resulting from the combustion of coal.  In this effort, a
 literature search was performed and over  300 separate refer-
 ences were studied. Information from other reliable sources
 and tests' was also utilized.

      As the gathering of information progressed, the most
 appropriate nomenclature and units were selected; thereafter,
 information covered was converted to the selected terms and
 standard units.

      Information required to support data  was often missing,
 and no data were used unless adequate supplementary informa-
 tion was available to justify whatever assumption had to be made
 in order for the data to  merit inclusion.
      In the process of organizing information, each possible
contaminant •was evaluated and the significance and interrela-
tionships of the quantities of materials present were carefully
studied.  The principal product of this effort was the establish-
ment of "emission factors. "  An emission factor is  the typical
value for the amount of a specific pollutant emitted.  Emission
factors were determined for pollutants from different types of
firing equipment and from different types of coal.

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      The information in this report is presented in the hope
that it will be useful in accomplishing the following purposes:

      1.  Development of community or area-wide inventories
         of emissions from coal combustion.

      2.  Evaluation of emissions from specific existing or
         proposed coal-burning installations where detailed
         data are not available.

      3.  Projection of the effects of coal combustion on the
         future air quality of communities.

      4.  Development and expansion of a central depository for
         emission data within the Technical Assistance Branch
         of the Division of Air Pollution.

      5.  Indication of the gaps in the knowledge and  understand-
         ing of the variables that influence emissions.

      6.  Dissemination of information on the effectiveness of
         various types of control equipment and processes.
                        EMISSIONS FROM COAL COMBUSTION

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                      CHAPTER  II.
        SUMMARY  OF  EMISSION DATA
      The mass emission rates of participates and gases arising
from the combustion of coal before stack gas collection is applied
are summarized in Tables 2-1 and 2-2, respectively.  The


       Table 2-1.  PARTICULATE EMISSION FACTORS
              FOR COAL COMBUSTION WI THOUT
                    CONTROL EQUIPMENT
               Type of unit
Particulate per ton
of coal burned, a Ib
      Pulverized
         General
         Dry bottom
         Wet bottom without
            fly-ash reinjection

      Wet bottom
         with fly-ash reinjection

      Cyclone

      Spreader stoker
         without fly-ash reinjection
         with fly-ash reinjectionb

      All other stokers

      Hand-fired equipment	
       16A
       17A
       ISA
       24A

        2A


       13A
       20A

        5A

       20
        The letter A on all units other than hand-fired
        equipment indicates that the percent ash in the
        coal should be multiplied by the value given.
        Example: If the factor is 17 and the ash content
        is 10  percent,  the particulate emission before
        the control  equipment would be 10 times 17 or
        170 pounds  of particulate per ton  of coal.

        Values should not be used as emission factors.
        Values represent the loading reaching  the control
        equipment always  used on this type of furnace.

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 factors are expressed as pounds of emission per ton of coal with
 a heat content of 13,000 Btu per pound.  The data are divided
 into three categories: (1) power plants (1 x 10^  Btu/hr input
 or more),  (2) industrial plants (107 to 108 Btu/hr input), and
 (3)  domes tic-commercial plants (107 Btu/hr input or less).  The
 factors in Tables 2-1 and 2-2 should not be used if the heating
 value of the coal used in an area varies significantly from
 13,000 Btu per pound.  Nomographs have been constructed to
 convert the emission values (or estimate emissions from a given
 unit) to those  appropriate for  the coal used in a particular area
 (Figures 2-1 and 2-2).

       The quality of the emission control effort within the area
 under study must not be neglected.  The estimate of particulate
 emissions for various degrees of control are generalized in
 Table 2-3.  If the emission without control is less than the value
 found in Table 2-3, the smaller number should be used.
    Table 2-2.  GASEOUS POLLUTANT EMISSION FACTORS
                   FOR COAL COMBUSTION
Pollutant
Nitrogen oxides
as NO2
Sulfur oxides
as SO
Carbon monoxide
Hydrocarbons
as methane
Aldehydes as
formaldehyde
Pollutant per ton of coal burned, Ib
Electric generating
plants
20
38 Sa
0.5
0.2
0.005
Industrial
plants
20
38 Sa
3
1
0.005
Domestic and
commercial plants
8
38 Sa
50
10
0.005
 S indicates that the percent sulfur in the coal should be multiplied
by 38.  Example:  If the sulfur content is 2 percent, the sulfur
emission would be 2 times 38, or 76 pounds of SO_  per ton of coal.
                         EMISSIONS FROM COAL COMBUSTION

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                                      PARTICULATE EMISSION,
REFERENCE lb/!06Btu 1 b/ 1031 b f 1 ue gas at
L| NE 5055 excess ai r
ASH
HEATING VALUE
I.OOOBtu/lb C0™,
20-t
18
1 O —

16 -

15 -
14-
13 -

12-

11 -
10-

9-

8-
7 -



6 -


5-









""" -- .
















-30


-20


-15


-IP.
9^

-8
-7
-6
-5
-4

-3

-2





-1
( Bituminous coal )
0.2-1
0.3-
0.4-
0.5-
0.6-

0.8-
A-i i-
*
'.

B 	 2 =

3-
C- 4-
E- 5n
M 6-
8-
10-
15-

20-
-0.2
-0.3

-0.4
-0.5
-0.6

-0.8
-1



-2

-3
-4
-5
-6
-8

-15

A. CYCLONE UNITS
B. ALL STOKERS OTHER THAN SPREADER STOKERS
C. WET BOTTOM, PULVERIZED, OR SPREADER STOKERS
WITHOUT FLY-ASH REINJECTION
D. DRY BOTTOM PULVERIZED
E. SPREADER STOKERS WITH FLY-ASH REINJECTION
F. WET BOTTOM PULVERIZED WITH FLY-ASH REINJECTION
     Figure 2-1.  Nomograph for estimating participate emissions from coal
            combustion  (without  air pollution control  equipment).
   Table Z-3.  ESTIMATES OF  CONTROLLED PARTICULATE

              EMISSIONS FROM COAL COMBUSTION
                     Particulate per ton of coal burned, Ib
Degree of
control
Average
Good
Electric generating
plants
25
10
Industrial
plants
25
15
Domestic and
commercial plants
25
20
Summary of Emission Data

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                                                  SOX as S02,
% SULFUR
IN COAL
10.0 -
 9.0 -
 8.0

 7.0 -

 6.0 ~


 5.0 ~


 4.0 -
 3.0 -
 2.0 --
 1.5  -
1 .0
0.9
0.8

0.7

0.6

0.5
                          HEATING VALUE,
                             Btu/lb
     ppm at
 5055 EXCESS AIR
(Bitumi nous coal )
             400'


             500-

             600-

             700.

             800-

             900-
           1.000-
                                                           Ib/IO6 Btu
                                -20,000

                                -15_,OPO -•
                                -5.000
                                                  1 ,500-E
                                                         r 4


                                                  2 ,000 -|- 5

                                                           6

                                                           7

                                                           8
                                                  3,000 - -
                                                  4..000--
                                                  5.000'

                                                  6,000•

                                                  7,000-
                                                  7,500•
                                                         -1 .5
                                                         '- 2
                                                         r 3
                    9

                    10
                 --15
                                                         - 20
         Figure 2-2.   Nomograph  for calculating SOX emissions.
                          EMISSIONS FROM COAL COMBUSTION

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                      CHAPTER III.

PROPERTIES AND  DISTRIBUTION  OF  COAL



INTRODUCTION

      During the geological ages vast deposits of vegetable ma-
terial accumulated to form the parent material of coal.  Through
many thousands of years this material underwent a process
involving changes in  temperature, pressure, submersion in water,
and biochemical action to form coal.  Although predominantly
carbon,  coal contains varying amounts of about half of the known
elements.  Coal is broadly classified as  (1) anthracite (hard
coal), (Z) bituminous (soft coal), or  (3) lignite  (brown coal).


COAL PRODUCTION AND DISTRIBUTION

      The U. S.  Geological Survey  estimates recoverable coal
reserves to be 830 billion short tons, the equivalent of 17. 3
quadrillion Btu of untapped energy.  The Department of Interior
reports coal underlying  350,000  square miles,  or approximately
one-ninth of the total area of the United States.  Bituminous coal
is mined  in 26 states, with West Virginia,  Kentucky,  Pennsylvania,
Illinois,  Ohio, Virginia,  Indiana, and Alabama,  in that order,
leading the tonnage output in  1963. 1  The United Spates produced
452 million tons of bituminous coal in 1963; 409  million tons  of
it was consumed in this  country. 1 Of the total energy from
fossil fuels and water power, coal supplies about 23 percent;
liquid petroleum,  41  percent; natural gas,  32 percent; and water
power,  4 percent.

      The bituminous and lignite fields iare organized into pro-
ducing districts  as defined in the  Bituminous Coal Act of 1937. 3
These districts  are shown in  Figure 3-1.  The anthracite fields
not included in the numbered producing districts are in Penn-
sylvania,  Rhode Island,  and Arkansas.

      Since the type of coal used in any area being studied is
important, it is  necessary to  have information on coal distribu-
tion "and utilization.   The Bureau of Mines^ publishes  data on
the distribution of bituminous coal and lignite in the various
states and geographic areas.  These data include the producing

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00
1
i
O


I
O
O
I
Figure 3-1.   Map  of the coal-produci nq  districts  of  the  United  States. 3

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 districts of origin,  method of transportation, and types of con-
 sumer use.  Table  3-1 shows the distribution of bituminous coals
 and lignite to the various states in 1962 from all districts of
 origin, and the percentage of coal supplied by each district.
 Tabulation of the amount of coal  produced in each district is
 shown in Table 3-2.

       Table  3-3 shows the distribution of coal among the various
 major users for the year 1963 and the predicted usage for 1975. *
 "Keystone Buyers Guide"^ contains a directory of fuel usage
 (including coal) for all major utilities in the United States; for
 all cement plants,  including  capacities; and a directory of bee-
 hive and by-product coke-oven plants with their capacities.
 Also helpful to the air pollution survey is the directory of the
 Retail Coal Merchants Association. ^  More complete data on
 the  amount of  fuel used by the electric  utilities can be found in
 the  National Coal Association publication "Steam-Electric Plant
 Factors. "6

       Analyses of coal used in producing districts  can be found
 in "Keystone Buyers Guide, "' as can typical analyses from
 seams within the various states.   The Bureau of Mines also
 publishes  coal analyses.  ' • °» °» *"
CHEMICAL PROPERTIES OF COAL

Classification of Coal
      The most common method of classifying coal is shown in
Table 3-4.  The criteria for the various classes of coals are
determined by "proximate analysis. "  This analysis  determines
the weight percent of moisture, volatile matter, fixed carbon,
and ash in a given coal, usually on an "as  received"  basis.  The
amount of moisture is determined by heating a coal sample  to
about 110°C for  1 hour; the  loss in weight  is then termed
"moisture. "  This same sample is then heated to 950°C for
7 minutes,  and the further loss in weight is called volatile
matter; it represents the hydrocarbons and other organics
driven off by the heat.   The remainder is fixed carbon and ash,
which are separated by combustion. H> 12

      Although the amount of sulfur, the heating value, and the
ash-softening  temperature are not part of the analysis, they are
usually reported with it. *•*  Table 3^5 lists typical ranges of
data from analyses of coals  used  in the United States. 13

Properties and Distribution  of Coal                           9

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                          Table 3-1.  DISTRIBUTION OF BITUMINOUS AND LIGNITE COAL IN 1962

                                          BY STATES  FROM PRODUCING DISTRICTS1' 3> 4
S

55
en
M

§
g

O
O
>
f
O

g
w
C!
CO
Region

New England

Mid-Atlantic

East N. Central


We. IN. Central




S. Atlantic



East S. Central




Mountain

Pacific
Canada
Mexico
Destination not
revaalable
State
Massachusetts
Connecticut
Maine. Rhode Uland, 1
New Hampshire, Vermont)
New York
lew Jersey
ennsy van a
Indiana
Illinois
Michigan
Wisconsin
Minnesota
tow a
Missouri
North Dakota)
South Dakota /
Nebraska, Kansas
Delaware , Maryland
District of Columbia
Virginia
West Virginia
North Carolina
South Carolina
Georgia, Florida
Kentucky
Tennessee
Alabama, Mississippi
Oklahoma, Texas I
Colorado
Utah
Montana, Idaho
Wyoming
New Mexico
Arlaona, Nevada
Washington, Oregon
California
Alatka



Total
market
in
thousand
ten*
4.342
4,047
1,608
21,737
6.901
'
31,624
39.259
27.255
5.766
5.047
7,685
2, 390
1,630
9.884
81
12,82
15.27
9,98
3,92

11.873
14, 120
16.716

3, 40
2, 17
1. 08
1. 38
07
488
964
1,426
893

i. 105

DUtrlct of origin in percent of total 1962 market*' b
1
24.4
31.0
9.9
30.3
29. 1

< 0.1
< 0. 1
1.0



38.6
30.6
0.3
0.1










0. 3


4.2

2
3.B
0.3
0. 1
16.2
4.9

< 0.1
< 0. 1
1.0



1.0


21.6













2.2

J
and
17.1
36.1
33.7
43.2
59.2

0.1
0.2
2.7


0, 4
39.2
1.9
0.1
25.3













1.3

4


1.6


< 0. 1
26.4






9.6













3. 1

7
5.9
4.4
2.2
0.9
2.6

12.4
2.5
7.2



7.6
27.4
11.4
7.4
6.2
2.8
0. 1
3. 3
2.7





1.2


25.6

9
48.8
28.2
54. 1
7.8
4.2

25.2
8. 1
53.6



3.6
0. 1
8.2
6.
3,
7.
4.
B.

0.2




0.4


31.8

9





16 1
11 2
2 6


0.1






26.2
49.4

2. 6







4.6

10





6 5
72 5
3 1

0. 3
0.8







28.8

1. 6







7.9

11





39.7
5.5
0.4




















2.0
















































19.1
3.9
81. 5
1. 2







12.7











0. 1









54. 6

7.0


0.5

100


with-
out







0.7
5. 0
35.0
0,2
81.4









37.2







4.6






















24. 4

















0. 2
0. 4
6. 5










65.3
11. 1
1. 3
15.0

29.9



























85.0
69.7
0. 3













12.0
10. 1








0 1

10.3
5.6
14.4
97.8

3.8













O.I
1.0










< 0. 1
76. 3
52.8
0.9
30. 3
69.6
69.3




21







12.6
81.7









2.5











22
and
23








0.4













32.8

24.7
100




               "Figure 3-1 ahows the location ol producing dlatrlcU in the continental United Statea.    ^Production from District S is negligible.

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     Table 3-2.  BITUMINOUS COAL PRODUCTION IN  1962
                      BY DISTRICT1'3'4
District number
and name
1 . E a s te rn P enns ylvania
2. Western Pennsylvania
3. Northern West Virginia
4. Ohio
5. Michigan
6 . Panhandle
7. Southern numbered 1
8. Southern numbered 2
9. West Kentucky
10. Illinois
1 1 . Indiana
1 2 . Iowa
13. Southeastern
14. Arkansas -Oklahoma
15. Southwestern
16. Northern Colorado
17. Southern Colorado
18. New Mexico
19. Wyoming
20. Utah
21. North-South Dakota
22. Montana
23. Washington
United States total
Production, thousand
net tons
30. 649
36,080
36, 516
34, 500

4, 475
33, 720
113,851
31, 300
, 48,400
15, 780
1, 150
15,934
924
4,406
790
3, 103
367
2, 570
4, 270
2,780
370
1,065
423, 000
Percent of total
production
7.2
8.5
8.6
8. 1
-
1. 1
8.0
27.0
7.4
11.4
3.7
0.3
3.8
0.2
1.0
0.2
0.7
0. 1
0.6
1.0
0.7
0.1
0.3
100
      From the air pollution viewpoint, the amounts of volatile
matter,  ash,  and sulfur and the heating value are the most
important part of the fuel analysis.  Volatile matter is related
to the emission of smoke, ^ the ash, to particulate emission;
and the sulfur content, to sulfur oxide emissions, whereas the
heating value is related to the total amount of pollutant produc-
tion.  Another coal variable connected with smoke and flue dust
emission is the size of coal.   The optimum size for coal is
determined by the method of firing and will be discussed in a
later section.

Typical Properties of Coal by Producing Districts

      The average sulfur contents of coals mined in this country have
been estimated at 2 percent for bituminous, and 0. 6 percent^, •'•"for
Properties and Distribution of Coal
11

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       Table 3-3.  BITUMINOUS COAL CONSUMPTION
  IN UNITED STATES FOR 1963 AND PREDICTED FOR 1975
Major user
Electric power utilities
Coking coals
Steel and rolling mills
Cement mills
Other manufacturing and
mining
Retail deliveries
Export
Motive power
Totals
Consumption in
1963,
millions of short tons
209.0
77.7
7.4
8. 1
83.5
23.5
47.1
-
456.3
Predicted consumption
in 1975,
millions of short tons
440
90
I 89
20
30
2
671
anthracite.  Several authors estimate that 10 percent ash and
2.5 percent sulfur are reasonable average figures for coal used
to produce electrical energy. 1°> *7  Of equal importance is the
range of volatiles, ash, and sulfur found in coal.  Such values
are presented in Table 3-6.  These values were calculated from
reference 8 and probably  are representative of the retail coal
sold from these districts, which are shown in Figure 3-1.

Coal Ash

      The ash-forming mineral matter in coal consists principally
of slate, clay,  sandstone, shale, carbonates, pyrite,  and gypsum.
Many other constituents occur  in trace amounts.  Table 3-7
shows the relative frequency of occurrence of the ash-forming
mineral matter in coal.   Typical ranges of coal-ash constituents
found in United States coal are presented in Table 3-8.
      Some mineral  matter  is derived from the soil above and
below the seam of coal being mined.  With the advent of mechan-
ical mining processes, the amount of mineral matter has in-
creased.  This and some  of the pyrites in the coal mav be
removed by washing or other mechanical processes.   '
Generally, coal shipped long distances  is of low-ash content
for economic reasons.  Also power plants usually burn higher-
ash coals,  whereas lower-ash  coals go to the retail market.
12
EMISSIONS FROM COAL COMBUSTION

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       Table  3-4.   CLASSIFICATION OF COALS BY RANK11
Class a
I. Anthracite
II. Bituminous e
III. Subbituminous
IV. Lignitic
Group
I. Meta-anthracite
2. Anthracite
3. Semianthracite
1. Low-volatile
2. Medium -volatile
3. High -volatile A
4. High-volatile B
5. High-volatile C
1 . Subbituminous A
2. Subbituminous B
3. Subbituminous C
1 . Lignite
2. Brown coal
Limits of fixed carbon or Btu
mineral-matter-free basis
Dry FCb 90% or more (dry VMC
2% or less)
Dry FC 92% or more and less than
98% (dry VM 8% or less and
more than 2%)
92% (dry VM 14% or less and
more than 8%)
Dry FC 78% or more and less than
86% (dry VM 22% or less and
more than 14%)
Dry FC 69% or more and less than
78% (dry VM 31% or less and
more than 22%)
Dry FC less than 69% {dry VM
more than 31%). Moist Btu^
14, OOflS or more
Moist1 Btu 13, 000 or more and
less than 14,0008
Moist Btu 11,000 or more and
less than 13,000^
Moist Btu 11,000 or more and
less than 13,0003
Moist Btu 9, 500 or more and less
than 11,0008
Moist Btu 8,300 or more and less
than 9, 5008
Moist Btu less than 8, 300
Moist Btu less than 8,300
Requisite physical
properties
Nonagglomerating
Either agglomerating
or nonweathering
Both weathering and
nonagglom crating
Consolidated
Unconsolidnted
  aStandard Specifications for Classification of Coals by Rank (ASTM D388-38, ASA M20.1-1938).
   This classification does not include a few coals that have unusual physical and chemical properties
   and that come within the limits of fixed carbon or Btu of the high-volatile bituminous and sub-
   bituminous ranks. AH these coals either contain less than 48 percent dry mineral-matter-free
   fixed carbon or have more than 15,500 moist mineral-matter-free Btu.
  bFC =  fixed carbon.
  CVM = volatile matter.
  **!£ agglomerating, classify in the low-volatile group of the bituminous class.
  elt is recognized that there may be noncaking varieties in each group of the bituminous class.
  fMoist Btu refers to coal containing its natural moisture, but not including visible water on the
   surface of the coal.
  SCoals having  69 percent or more fixed carbon on the dry mineral-matter-free basis shall be
   classified according  to the fixed carbon,  regardless of Btu.1
  "There are three varieties of coal in the high-volatile C bituminous coal group, viz., variety 1,
   agglomerating and nonweathering; variety 2, agglomerating and weathering; variety 3, non-
   agglomerating and nonweathering.
        An apparent linear relationship  exists between the heat
content and  the ash  content (both on a  dry basis).   This  relation-
ship is  shown in Figure  3-2.   For clarity, the individual  points
have been  deleted.   The accuracy of each line  is about plus or
minus 10 percent.
Properties and  Distribution of Coal
13

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      Table 3-5.  RANGES OF VALUES FROM ANALYSES
          OF COALS USED IN UNITED STATES13

Moisture, weight %
Volatile matter, weight %
Ash, weight %
Sulfur, weight %
Heating value, Btu/lb
Bituminous
2-15
14-40
4-15
0.5-4.5
11,000-14,000
Anthracite
4-10
4-8.5
7-20
0.4-0.8
11,000-13,500
      One would expect a direct relationship between ash content
and particulate  emission; but as shown by the data in Figure 3-2,
this  is not the case.  A 100 percent increase in the ash content
decreases the heating content 5 to 15 percent;  the resulting
increase in particulate emissions is 110 to 130 percent.
Sulfur in Coal

      Sulfur occurs in coal in three forms:  pyritic, organic,
and sulfate  sulfur.  The proportions of each sulfur compound
vary widely.  The amount of sulfur as sulfate is usually small
in freshly mined coal.  The pyritic sulfur is found in small,
discrete particles within the coal,  and a percentage of this
sulfur may  be removed by washing or other mechanical means.
The organic sulfur is usually evenly distributed'throughout the
coal and cannot be removed without changing the chemical
nature of the coal. 18

      Although there is no definite relationship, sulfur has been
found to be  a contributing factor in the formation of clinkers and
slag in stokers.  A study conducted by the Bureau of Mines
showed that Pennsylvania coals with high ash-softening tem-
peratures usually have a low sulfur content.  This, however,
does not mean that low ash-softening-temperature coals have
high sulfur  content, as shown in Figure  3-3. HI 20

Chlorine in Coal

      As noted in Table 3-7, various salts are  found in coal
mineral matter.  Some of these salts are chlorides, such as
potassium and sodium chlorides.  Until  the last decade, this
14
EMISSIONS FROM COAL COMBUSTION

-------
TJ
i-t
o
V
a>
(D
in


B
o
H"'
0)
I-t-
H
H-
CT1
H-



§
O
o
Table 3-6.  SELECTED PROPERTIES OF UNITED STATES COALS


                 BY PRODUCING DISTRICTS,  19618


                      (Analysis on a dry basis)
Producing
district
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
Pennsylvania
(anthracite)
Volatile matter, %
Low
15.5
32.3
27.7
32.6

36.3
12.5
21.8
39.8
37.8
40.7
38.8
27. 1
21.8
31. 1
37.7
29.5
44.4
41.6
40.0
38.8
34.7
38, 1
3.5
Average
25.9
35.8
37.3
41.3

38.8
21.0
34.0
42.6
42.4
43.6
42.7
31.4
24. 1
38.1
38.1
37.6
44. 5a
42.8
43.2
42.8
38.2
39. 9a
5.9
High
39.5
42.6
42.7
46.2

43.3
25.9
42.6
47.3
48.3
45.9
45.0
39.5
30.4
44.6
38.5
42.6
44.5
44.4
48.7
49.7
41.6
41.6
9.4
Ash, %
Low
7.4
6.9
2.3
3.8

4. 1
2.5
1.5
5.5
6.0
6.9
10.8
1.7
5. 1
4.3
5.2
6.3
7.5
3.5
4.3
9.8
7.1
9.1
6.4
Average
8.8
9.7
7.3
10.4

6.4
5.7
6.7
7.9
9.6
9.0
16.1
8.3
8.9
8.9
6.4
8.7
7.8a
5.9
6.3
13.3
9.5
12.2
11. 1
High
20.2
19.1
12.0
26.1

8.7
31.7
18.4
12.6
13.5
11.2
22. 1
17.0
12.0
13.2
7.9
14. 1
8. I
7.6
8. 1
22.7
12.6
15.8
15.8
Sulfur, %
Low
1.0
0.9
0.6
1.9

0.6
0.6
0. 1
2.8
2. 1
1.0
5.0
0.6
1.2
0.6
0.3
0.4
0.8
0.5
0.3
0.9
0.5
4.9
0.4
Average
1.8
2.1
1.8
3.9

1.7
0.8
1.2
3.5
3.3
3.3
6.4
0.9
2.7
2.3
0.4
0.7
0. 9a
0.6
0.5
1.5
0.9
4. 9b
0.6
High
4.5
4.2
3.7
9.4

4.0
1.6
4. 5
4.8-
4. 4
4.2
8.0
2.2
3.2
5.6
0.4
1.2
0.9
0.8
1.0
1.8
1.4
4.9
1.4
Heat content, Btu
Low
11,770
13,220
13,000
10,330

13,730
10,240
12,230
12,490
12,700
12,870
10,690
12,340
13,550
12,450
12,380
12, 150
13,010
12,120
13,290
9,490
10,580
10,890
12,360
Average
14,100
13,650
13,850
13,000

14,200
14,800
14, 100
13,400
13, 100
13,190
11,700
12,800
14, 100
13,600
12,460
13,280
13,050a
12,500
13,600
10,600
12,200
12,000
13,300
High
14,580
14,290
15, 180
14,800

14,690
15,390
15,380
13,940
13,760
13,580
12,490
14,940
14,650
14, 380
12,620
14,230
13,080
13,220
13,900
11,000
12,870
12, 920
14,250
              Two samples.
            One sample.

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    Table 3-7.  RELATIVE FREQUENCY OF OCCURRENCE

                   OF MINERALS IN COAL19

Mineral
Clay and shale
11 lite
Sericite
Montmorillonite
Kaolinite
Halloysite
Sulfides, Sul fates
Pyrite
Marcasite
Sphalerite
Chalcopyrite
Galena
Pyrrhotite
Barite
Gypsum
Carbonates
Siderite
Ankerite
Calcite
Dolomite
Oxides, hydroxides
Hematite
Quartz
Magnetite
Rutile
Lirnonite
Goethite
Diaspore
Phosphate
Apatite
Silicates
Zircon
Biotite
Staurolite
Tourmaline
Granite
Epidote
Orthoclas e
Augite
Hornblende
Cyanite
Chlorite
Salto
Halite
Sylvite
Melanterite
Alunogen
Kieserite
Bischofite
Glaubers salt

Formula

KNaO 3AI203- 6S»O2- 2H2O
KNaO- 3MeO- A12O3 - 24SiO2 • 12H2O (Me = Fe, Ca, Mg>
Al2O3-4SiO2-nH2O
Al2O3'2SiO2'2H2O
Al2O3'2SiO2'4H2O

FeS2
FeS2
ZnS
CuFeS2
PbS
FeS
BaSO.
CaSO4- 2H2O

FeCO,
CaFe(C03)2
CaC03
CaMg
-------
14
12
  0
      NOTE:  NUMBERS SIGNIFY
      PRODUCING DISTRICTS,
    - DISTRICTS 5 AND 23  NOT
      SHOWN  BECAUSE OF IN-
      SUFFICIENT DATA.
10,000     11,000    12,000    13,000    14,000   15,000   16,000
                    COAL  HEATING VALUE (DRY BASIS), Btu/lb
   Figure 3-2.  Relationship between ash content and heatinq value of coal
                     from various producing districts.
Properties and Distribution of Coal
17

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           Table 3-8. TYPICAL LIMITS OF COAL
                 ASH IN UNITED STATES19
Constituent
Silica, SiO
Lj
Alumina, Al O
Ferric oxide, Fe O
b J
Calcium oxide, CaO
Magnesium oxide, MgO
Titanium oxide, TiO
Li
Alkalies, Na_O + K O
Sulfur, as SO
Weight percent
20-60
10-35
5-35
1-20
0.3-4
0.5-2.5
1-4
0.1-12
      Table 3-9.  CHLORINE CONTENT OF SELECTED
                   AMERICAN COALS19
            Source of coal
State
Ohio
Illinois
Indiana
West Virginia
Pennsylvania
Illinois
Oklahoma
Bed
Sharon
No. 6
No. 4
Pittsburgh
Lower Freeport
Central Illinois
Henryetta
Chlorine content, %
0.01
0.01
0.06
0.07
0. 14
0.35
0.46
18
EMISSIONS FROM COAL COMBUSTION

-------
        O
        o
UPPER LIMIT OF
RELATIONSHIP
                 J| RANGE'OF VALUES!!!;
                 vm;.;i;:;;::m m^m^ms
               LOWER LIMIT
             Q|OF RELATIONSHIP
             2,000    2,200    2, TOO    2,600    2,800    3,000
                    SOFTENING TEMPERATURE OF ASH,°F

           Figure 3-3.  Relation between percentaqe of sulfur in
           Pennsylvania coals and ash-softeninq temperature.''1^

 PHYSICAL PROPERTIES OF COAL
 Coal Sizing

       Commercially,  coals are referred to by such terms as
 "run of mine, " which is unscreened broken coal from the mine-
 "slack coal, " which is all the coal passing through a screen of'
 a given size,  such as  1- or 2-inch slack; and double-screened
 sizes,  such as "egg," "stove," "nut," "pea," and "stoker."12
 For anthracite,  the double-screened sizes are standardized,
 and the names, such  as "egg," refer to a definite size
 (Table 3-10).  For other coals, however, these terms  are just
 trade names,  having no fixed meaning unless  they are accom-
 panied by the numerical sizes. 10 Table 3_n Ustg several
 sizes of bituminous coal and their most common use.
Fusibility of Coal Ash

      One important property of coal ash is the "ash-softening"
or "fusion" temperature.   This is the temperature at which the
coal ash softens and fuses.  The composition of the ash deter-
mines the ash fusion temperature  (Table 3-12).  In general,
mixtures high in silica or alumina,  or low  in pyrites usually
have a high fusion temperature.  A coal high in pyritic sulfur
is necessarily high in iron; the possible resultant lower silica-
iron ratio lowers the fusion temperature. H.21  (See Figure
Properties and Distribution of Coal
                                                             19

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N>

O
Table 3-10.  STANDARD SIZING OF PENNSYLVANIA ANTHRACITE APPROVED AND


             ADOPTED BY ANTHRACITE INSTITUTE,  APRIL 1,  193121


                               (Round-mesh screen)
Name


Stove 	

Pea 	
No. 1 Buckwheat 	
No. 2 Buckwheat (rice)
No. 3 Buckwheat (barley)
Breaker rnesh, in.
4.1/4 . 4-1/2
3-1/8 - 3-3/8
2-3/8 - 2-4/8
1.-9/16 - 1-11/16
24/32 - 27/32
17/32 - 19/32
9/32 - 11/32
6/32 - 7/32
3/32 - 4/32
Test mesh, in.
Through
4-3/8
3-1/4
2-7/16
1-5/8
1-3/16
9/16
5/16
3/16
M
V
>
O
3-1/4
2-7/16
1-5/8
1-3/16
9/16
5/16
3/16
3/32
Oversize maximum, %
5
5
5
5
10
10
10
10
Undersize, %
Maximum
15
15
15
15
15
15
15
20
Minimum
7-1/2
7-1/2
7-1/2
7-1/2
7-1/2
7-1/2
7-1/2
10
Maximum
impurities , %
o>
•M
rt
a
1-1/2
1-1/2
2
3
5

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   Table 3-11.  GENERAL USES OF SEVERAL BITUMINOUS
                         COAL SIZES
                                     11
        Type
                                    Most common use
        5 lump

      5x2  egg

    2 x  1-1/4 nut


  1-1/4 x 3/4 stoker

 1-1/4 x 5/16 stoker

   3/4 x 3/8  stoker

    3/4  x 0  slack
    5/8  x 0  slack

    1/2x0  slack

    1/4x0  slack

1-1/4 x  0 nut and slack
    2x0 nut and slack
Hand-firing, domestic and industrial

Domestic hand-firing and gas producers

Domestic hand-firing, industrial stokers,
   and gas producers
Domestic and small industrial stokers

Domestic and small industrial stokers

Domestic and small industrial stokers

Industrial stokers and pulverizers

Particularly suited to pulverizers

Particularly suited to pulverizers

Particularly suited to pulverizers

Industrial stokers

Industrial stokers
 Coking and Caking Properties of Coal

      Coke is the fixed carbon and ash, which are left after the
 coal has been heated and the volatile matter has been driven
 from it.  In this sense,  all coals coke; however, the term
 "coking coal, " which is  used synonymously14with "caking coal, "
 refers  to a coal that melts and fuses to form, larger lumps, even
 though  the coal  may have been in small pieces.  Thus,  the caking
 process takes place to varying degrees and is described by
 various adjectives, such as "strongly  caking,"  "weakly caking,"
 or "non caking" coals.  A free-burning coal is the same as a
 noncaking coal. ^ Bituminous is usually  a caking coal, whereas
 anthracites and most subbituminous coals are free-burning coals.
 Properties and Distribution of Coal
                                   21

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         Table 3-12.  ASH-SOFTENING TEMPERATURES AND ASH COMPOSITION OF SELECTED COALS20
Sample
Montana subbituminous
Illinois bituminous
Pennsylvania bituminous
West Virginia semibituminous
Kentucky bituminous
Softening
temperature,
°F
2,060
2,320
2,500
2,730
> 2,900
Analysis of ash, %
Si02
30.7
46.2
49.7
51.0
58.5
A12°2
19.6
22.9
26.8
30.9
30.6
Fe2°3
18. 9
7. 7
11.4
10.7
4.2
TiO
LJ
1. 1
1.0
1.2
1.9
1.8
CaO
11.3
10. 1
4.2
2.1
2.0
MgO
3.7
1.6
0.8
0.9
0.4
Na O + K O
LJ £*
2.4
1.5
2.9
1.4
1.6
so3
12.2
8.9
2.5
0.6
0.9
 w
§
CO
g
n
o
n

i
td
c!
CO
§

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                     CHAPTER IV.
        COAL  COMBUSTION THEORY
COMBUSTION OF COAL

      The heating value of coal is principally a function of its
carbon and hydrogen content.  In order for heat to be released,
the coal must be  oxidized, or burned.   The process is a chemi-
cal reaction of carbon and hydrogen with oxygen (from the air)
that forms carbon dioxide and water, and releases heat; however,
several necessary conditions must exist before this reaction can
take place.  For  the reaction to go to completion, there must be
an excess of oxygen in the presence of proper temperature and
turbulence of the combustion gases for  a necessary period of
time.

      Coal will not burn as a solid; no fuel will.  The combustion
process must vaporize, gasify,  or break down a  solid into indi-
vidual molecules by the addition of heat.  When coal burns in a
bed on a grate, the  incoming or primary air through the grate
is heated by the  ash or burning fuel.  As the air temperature
rises, the heat begins  to vaporize and scrub off volatile and
carbonaceous material from the coal particles.   In this vaporous
state, the combustible material is oxidized. 23, 24  jn suspension
firing, a similar process takes place, with the energy of the
flowing gases replacing the function of the grate.-
      Air is approximately 21 percent oxygen and 79 percent
nitrogen by volume.  As air travels through a bed of fuel,  oxygen
is consumed by combustion, the oxygen concentration is reduced,
and the possibility of oxygen contacting the  fuel decreases.
Because of the lack of oxygen,gases leaving the bed carry  with
them a high concentration of carbon monoxide and other com-
bustible matter.  Above the bed,  more air (secondary air) must
be introduced  to oxidize all of the combustible material. Nitrogen
from the air tends to dilute and prevent contact between oxygen
and combustibles.  To overcome this effect, in a reasonable
period of time, there must be an overabundance or excess of air;
in other words,  an increase of air over and above the chemically
required (stoichiometric) amount.  The amount of excess  air
needed varies for each type of furnace (see chapter 5).

                              23

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      To increase the amount of contact of oxygen with the
combustible material,  a high degree of turbulence must be main-
tained.  Turbulence reduces the amount of excess air necessary
for complete combustion.  Figure 4-1 compares  the flue gas
analysis for poor mixing to that of ideal mixing.  With ideal
mixing,  the theoretical air-to-fuel ratio is all that is necessary
to achieve complete combustion.  As the mixing becomes less
ideal, excess air is needed to completely burn the combustible
matter.
                                                  POOR MIXING

                                                  IDEAL MIXING
               DEFICIENCY   ^     EXCESS AIR
                     CHEMICALLY CORRECT

                          AIR-FUEL RATIO
      Figure M~i.  Effect of ai r-fuel  ratio on flue aas analysis.25
      It might seem logical to assume that the primary function
of a furnace is to attain 100 percent combustion.  This, however,
is not true.  The primary purpose is to help attain the highest
overall efficiency for the energy system.  Usually this means
the point at which the most steam is raised for the least amount
of coal.  Starting from the low side, an increase in excess air
will usually increase  the combustion efficiency while at the same
time diluting and cooling the combustion gases.  After a given
point,  more heat is lost in the stack gases by the increase in
excess air than is gained by releasing the remaining heat-of
combustion.  This point would be that of maximum overall
thermal efficiency (Figure 4-2).  Usually, from 0.5 to 5 percent
of the thermal energy of the fuel is sacrificed  for optimum
operation. ^°
24
EMISSIONS FROM COAL COMBUSTION

-------
     iS
     O (/)
     (J <
       UJ
     Q a
     LJ U
     z z
     ce. —
     OQ
                        INCREASING EXCESS  AIR-
    (J ID
    U- O)
    LL) <
      LJ
    -I K
    -i a
    < z
    CC —
                                     MAXIMUM OVERALL
                                     EFFICIENCY
                      INCREASING  EXCESS AIR

       Figure 4-2.  Effect of excess air on combustion efficiency.



COMBUSTION IN FUEL BEDS

      When coal is burned 3n grates, one of two types of feeding
mechanisms is generally  used, overfeed or underfeed.  The
overfeed operation introduces  coal to the grate from the top and
the primary air under the grate,  and burning occurs from the
bottom to the top of the fuel bed.   The underfeed operation intro-
duces  the primary air and the  fuel from below the grate, and
the fuel burns from the top to the bottom of the bed.  There is
also a third operation called cross-feeding, which is a com-
bination of the two types.  H»2?
Coal Combustion Theory
25

-------
      The  idealized overfeed fuel bed is a series of layers,
which merge into each other as shown in Figure 4-3.  At the
bottom  of the bed and above the grate, a layer of ash serves
to protect  the grate and to preheat  the primary air.   The ash
layer merges into the actively burning oxidation zone.  Here,
the distilled coal undergoes the exothermic reaction,
C  + O2  =  CC>2,  which consumes almost all of the oxygen
from the primary air.   This is the hottest part of the fuel bed
with temperatures above 3,000°F.   Above this is a reduction
zone where, in the presence of high temperatures and a high
concentration of CC>2, an  endothermic reaction,  CC>2 + C =  2CO,
reduces the temperature of the gases and the fuel bed.   The top
layer is the distillation zone where volatile matter is distilled
off the fresh or green coal.  12,24,27,28

      Figure 4-3 shows the  relative concentrations of the
various  combustion gases and the temperature as the gases
travel through the bed.

      That part of the bed termed "ignited fuel"  contains both
the oxidation and reduction  zone.  As shown by the relative
concentration curves next to the  diagram, the two zones blend
together with no  definite division.
                     RAW
           COMBUSTION FUEL
           GASES  A   JlL
         TEMPERATURE
     IGNITION_
     PLANE
        GRATE
         0      10    20     30
        COMPOSITION . % by volume
                  PRIMARY
                  AIR
   Figure t-3.  Idealized overfeed fuel bed and relative distribution of
                temperature and products of combustion. 28
26
EMISSIONS FROM COAL COMBUSTION

                            GPO 825-629—3

-------
      The underfeed fuel bed is  the reverse of the overfeed
operation (Figure 4-4).   Raw fuel is fed in from the bottom
above the grate and under the actively burning coal.  Incoming
air below the grate enters the bed, is  heated,  and distills
volatiles from the  coal.  This mixture of volatiles and oxygen
rises to the ignited zone, where it first oxidizes the carbon
and hydrogen in the volatile matter, and then reduces the CO2
to CO as the gases travel upward.  On top of the bed is the
ash.24'27'28^
                                 TEMPERATURE-
       I GN I T I ON-
          PLANE

          GRATE
                                  CO
                                               CO
 0     10    20    30
COMPOSITION, %  by volume
                    i TED' FUEL"
V#xRAW' FUEL •#:
                   RAW    A I R
                  FUEL
   Figure 4-M-.  Idealized underfeed fuel bed and relative distribution of
                temperature and products of combust ion .28
      After the primary air has passed through either the over-
feed or underfeed fuel bed, virtually all of the oxygen has
combined with the carbon to produce CO and CO£.   The gases
leaving the fuel bed are rich in volatile hydrocarbons and tars,
carbon monoxide, and nitrogen.  Unless secondary air is intro-
duced,  these hydrocarbons and tars crack,  decompose, or
condense,  and are emitted to the atmosphere as a white,
yellow, or black smoke. 12,24,27,28  Black carbon is not
produced by gases coming in contact with cool heating surfaces,
but is formed at or near the surface of the fuel bed.
      The velocity of the combustion reaction is faster than the
velocity of decomposition.  If oxygen is present in sufficient
quantity at the time  of distillation, hydrocarbons oxidize com-
pletely without forming soot and smoke through thermal crack-
ing and condensation reactions.  For this reason, secondary
air should be  admitted as near the surface of the fuel bed as
Coal Combustion Theory
                                             27

-------
possible and should have sufficient velocity to penetrate to the
combustion zone so that oxygen is available for completing the
combustion reaction. ^9

      For  the  combustion process to  take place,  sufficient  heat
must be provided for  each  fuel component to reach the "self-
ignition" temperature  and sufficient air must be available  to
supply the necessary oxygen.     If a given combustion temper-
ature is maintained and primary air  is decreased, the burn-
ing rate in the fuel bed is  decreased.  In practice,  the main
method of controlling  the burning rate is by the regulation of
the primary air.   Secondary air  controls the efficiency of the
combustion over the fuel bed.   The depth or thickness of the
fuel bed does  not control the burning rate to any  great extent;
however,  it  does  control the amount  of carbon  monoxide leav-
ing the top of the  bed.  A thick bed produces higher  concen-
trations  of carbon monoxide because  of the larger reduction
zone.12'24'27
COMBUSTION OF COALS IN SUSPENSION


      Combustion of coal in  suspension is  similar in principle
to combustion in an overfeed fuel bed.  The volatile matter
is first distilled off and burned; the fuel particle is thus sur-
rounded by a highly reducing atmosphere.   Secondary air and
sometimes highly turbulent gases move the reducing atmos-
phere  away so that more oxygen comes in  contact with the
particle for  complete combustion.   For some suspension-fired
units,  such as the  spreader  stoker, final oxidation takes
place on grates, whereas in pulverized-coal-fired and cyclone
units,  complete  combustion takes place in the suspended fuel
bed.12

      Various arrangements for  suspension-fired units are shown
in Figure  4-5.
28                     EMISSIONS FROM COAL, COMBUSTION

-------
             FANIAIL       MULIIPLE  INTERIUBE

                (a) VERTICAL FIRING
                                                            PRIMARY AIR
                                                            AND COAL

                                      5
                                      SECONDARY
                       PLAN VIEW 01 (URNACE

                        f   IANGEN1I AL  FIRING
                           PRIMARY AlR
                           AND COAL
               Vcl
                       SECONDARY AIR
             MULTIPLE INTERIUBE
                  i'rt ;M/. ;• Y ;. j i
                  ..«  CO/.L
                SECONDARY Al R _J

                           CIRCULAR

(c)  HORIZONIAL  FIRING
         SECONDARY AlR
       PRIMARY A IR
       AND COAL
         CYCLONE•


           (d) CYCLONE  FIRING
                                          AND COAL
                      (c) OPPOSEO-INCLINEO F IRING
         Figure 4-5.   Various  methods  of firing coal  in suspension.
                                                                           12
Coal Combustion  Theory

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                      CHAPTER V.
              HOW  COAL IS  UTILIZED
BRIEF HISTORY OF DEVELOPMENT OF MECHANICAL
FIRING METHODS

      The widespread use of mechanical firing has been a major
factor in reducing the visible smoke plume from coal-fired
boilers  and furnaces.
      Underfeed stokers of various designs were built before
1900, with major improvements being developed as early as
1906.  Both single- and multiple-retort units were being
installed at that time.  Chain-grate and traveling-grate stokers
were introduced between 1900 and 1920; the first forced-draft
units were made in 1922.   Although spreader stokers of crude
design were manufactured in the early 1900's, they did not
become a successful firing unit until  about 1925.  Their popu-
larity increased rapidly in the 1930's. 2^, 31
      The development of the small underfeed stoker for home
boilers and furnaces in the early 1930's made automatic coal
firing available to every coal user, regardless of size of
equipment.
      Pulverized-fuel firing was first applied to boilers for
steam generation in 1920 and has progressed in development.
Cyclone furnaces appeared about 1947.  Today pulverized-coal
burners and cyclone furnaces are the universal methods of
firing coal in the new large electric-generating stations.
      The newest entry into the firing equipment field is the
vibrating-grate stoker, which has been applied to large industrial
boilers since about 1954.  This type of firing unit, utilizing a
water-cooled inclined grate, has been the focal point in the
development by Bituminous Coal Research of a small-to-medium-
sized, completely packaged boiler.

                               31

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DESCRIPTION AND SIZE RANGES OF MECHANICAL
FIRING EQUIPMENT24- 31, 33
Underfeed Stokers,  Single-Retort,  Residential

      In the residential underfeed stoker, the coal is fed from
a hopper or directly from the coal  storage bin to the retort by
a continuous, rotating screw (see Figure 5-1).  Coal rises
into the firing zone  from underneath, thus the term "underfeed
firing. "  Air  is delivered to the firing zone through tuyeres
(grate openings), also from underneath the actively burning bed.
The coal and  primary air control is "all on" or "all off. " Ash
is removed as a clinker from a refractory hearth through the
furnace firing door.   Burning rates range from 1  to 60 pounds
of coal per hour.
                    FIRE BOX

                     BURNER HEAT
               Figure 5-1.   Residential underfeed stoker


Underfeed Stokers, Commercial,  Institutional,  and Small
Industrial

      The general arrangement is  as described  in the previous
paragraph, with "dead" plates replacing the refractory hearth
(Figure 5-2).  As sizes become larger,  screw feeders are re-
placed by a mechanical ram, which feeds coal to pusher blocks
that distribute the coal in the fire box.  Ash is discharged by
side-dump grates.  Modulating combustion controls, i.e., vari-
able control of both fuel and air  rates, are often used.  Forced
draft is automatically regulated,  and separate over fire-air sys-
tems  are  used, particularly when  on-off controls are used.  A
 32
EMISSIONS FROM COAL COMBUSTION

-------
 bridge wall retains the coal over the stoker grates.   The size
 ranges for screw-feed stokers are 60 to 1, 200 pounds of coal per
 hour and for ram-feed stokers ,  from 300 to 3 , 500 pounds per hour.
                      ••^'TRANSVERSE SECTION
                                       w
                           LONGITUDINAL SECTION
             Figure 5-2.  Single-retort underfeed stoker.
Multiple-Retort Underfeed Stokers

      As the name implies,  these units usually consist of
several inclined retorts side by side, with rows of tuyeres in
between each retort (Figure 5-3).  Coal is worked from the
front hopper to the rear ash-discharge mechanism by pushers.
The forced-air system is  zoned beneath the grates by means
of air dampers, and the combustion control is a fully modu-
lating system. In the larger furnaces the walls are water-
cooled, as are the grate surfaces in some units.   Multiple-
retort underfeed stokers are losing their  popularity, giving
way to spreaders  and  traveling-grate units.  Sizes range
from 20, 000 to 500, 000 pounds of steam per hour with burning
rates up to 600, 000 Btu per  square foot of grate per hour.
Traveling-Grate and Chain-Grate Stokers

      Traveling-grate and chain-grate units (Figure 5-4) are
essentially moving grate sections, moving from the front to the
rear and carrying coal from the hopper in front through a gate
How Coal is Utilized
                                                            33

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                                             COAL HOPPER
                                                 f COAL  RAMS
                     ASH-
                DISCHARGE PLATE
              FUEL
          DISTRIBUTORS
                 Figure 5-3.  Mul t i pi e-retort underfeed stoker.
                                     OVERFI RE-AIR
                                      NOZZLES
                       AIR-CONTROL
                         DAMPERS
                       ,  L/AHrcno  *
-RETURN
 BEND
              m BTB STQ flTG HVQ fl^CT ^STtt 6jTfl flTfl ATfl tflTn mfl AfiSl WH »!U

                   	   1
                            DRAG
                            PLATE
              STOKER
              CHAIN
 DRIVE
SPROCKET
HYDRAULIC
 DRIVE
             Figure 5-4.  B &  W jet-ignition chain-grate stoker.
into the combustion zone.  The fuel bed burns progressively to
the rear,  where the ash is continuously discharged.   Older
units with natural draft are fast disappearing; modern units  have
zone-controlled forced draft.  Complete combustion-control
systems are utilized, and overfire air, especially in the  front
wall,  is an  aid to burning the volatiles in the fuel.  Units range
in size from 20 to300xl(PBtu per hour input.
34
EMISSIONS FROM COAL COMBUSTION

-------
Vibrating -Grate Stoker

      This unit consists of a water-cooled grate structure on
which the coal moves from the hopper at the front of the boiler
through the burning zone by means of a high-speed vibrating
mechanism automatically operated on a  time-cycling control
(Figure 5-5).  As in the traveling grate,  the fuel bed progresses
to the rear,  where the ash is continuously discharged.  Forced
air is zone-controlled and regulated, along with the complete
coal and air system,  through an automatic combustion-control
regulator.  Grate heat release may range from 350, 000 to
500, 000 Btu per square foot per hour.  The size range  for this
unit is  from 5,000 to 100,000 pounds of  steam per hour.
                                                  COAL HOPPER-
                                                COAL GATE-
                                      OVERFI RE-AIR NOZZLES
              Figure 5-5.  Vi brat i nq-qrate stoker  furnace.
BCR* Automatic "Packaged" Boiler
      This unit is a complete steam or hot water generating
system,  incorporating a water-cooled vibrating grate as the
firing mechanism (Figure 5-6).  Coal is delivered from the
storage bin to a hopper from which it travels on the vibrating
grate to  the fuel bed.  Ash is discharged automatically with
a screw  conveyor.  The unit has completely automatic com-
bustion controls so that coal feed to the hopper from the bin
and ash discharge is coordinated with load conditions.  Forced
and induced draft  fans are used.  The size range is from 3 to
20 million Btu per hour input.
^Bituminous Coal Research,  Inc.
How Coal is Utilized
                                                            35

-------
        FLUE GAS
        EXHAUST
                       -STEAM
        Figure 5-6.  Bituminous Coal Research,  Inc., packaged boiler
Spreader Stoker

      The spreader stoker combines suspension and fuel bed
firing by the stoker mechanism feeding from the hopper onto
a rotating flipper mechanism,  which throws the fuel into the
furnace  (Figure 5-7).  Because fuel is burned partly in sus-
pension  and partly on the grate,  the fuel bed is  thin, and
response to fluctuations  in load is  rapid.  The grates are
either stationary or continuously moving from the  rear to the
front.  Vibrating, oscillating,  traveling, and chain grates are
designed for moving the  fuel toward the ash receiving pit.
                                                   GRATE
                Figure 5-7.  Spreader stoker-fired  furnace.
36
                         EMISSIONS FROM COAL COMBUSTION

-------
      Zoned undergrate air is important, as is the careful
application of a responsive combustion control system.  Over-
fire air is necessary.  Fly-ash carryover is strongly influenced
by high burning rates,  whereas smoke  emission is increased
at low burning rates.  In large units, cinders are often returned to the
grate from the fly-ash collector to reduce unburned carbon losses.
Spreader stokers range in size from 6  to 500 x 1CP Btu per hour
input or from 5, 000 to 400, 000 pounds  of steam per hour output.


Pulverized-Fuel Firing Units

      In this system,  coal is pulverized to particles,  at least
70 percent of which pass through a 200-mesh sieve,  and is
fired in burners similar to those used for liquid fuel (Figure 5-8).
In direct-firing systems,  raw coal is dried and pulverized simul-
taneously in a mill and is fed to the burners as required by the
furnace load.  The control system regulating the  flow of both
coal and primary air is so designed that a predetermined air-
coal ratio  is maintained for any given load.  The  indirectly fed
unit utilizes storage bins  and feeders between  the pulverizers
and the burners.  Some bin-and-feeder systems are in  use, but
the majority of plants use direct-firing units.
                           Radiant superheater
                                    Convect ion
                                    superheater

                                    Economi zer
                                     Ai r heater
                  Figure 5-8.
Pulveri zed-coal-fi red
 uni t.
      Burners are characterized by their firing position,
i. e. ,  horizontal, vertical,  or tangential.  Arrangements for
the introduction of primary, secondary,  and, in some cases,
tertiary air vary with burner manufacturers.  One manufacturer
How Coal is Utilized
                                                             37

-------
uses an adjustable burner, which is tilted upward or downward
to control the furnace outlet temperature, so that steam temper-
ature can be regulated over a wide range of capacities.

      Pulverized-coal-fired units  are usually one of two basic
types, wet bottom or dry bottom.   The temperature in a wet-
bottom furnace is maintained  above the ash fusion temperature,
thus the slag is melted so that it can be removed from the
bottom as a liquid.  The  dry-bottom furnace maintains a temper-
ature below this point so that  the ash will not fuse.

      Pulverized-fuel-fired boilers range in capacity from
200, 000 to several million pounds of steam per hour.


Cyclone Furnace

      The cyclone furnace  is a water-cooled horizontal cylinder,
in which the fuel is fired and heat is  released at an extremely
high rate for the given volume (Figure 5-9).  Coal is  crushed
so that approximately 95 percent passes  through a 4-mesh
screen.  Coal  is introduced into the burner end of the cyclone,
and air for combustion is admitted tangentially.  Combustion
occurs at heat-release rates of  500, 000 to 900, 000 Btu per
cubic foot per  hour at gas temperatures sufficiently high to
melt a high percentage of the  ash into a liquid slag, which is
discharged from the bottom of the furnace through a slag tap
opening.  The  size range of boilers fired are comparable to
those with pulverized-fuel  units.
            SCREENED-FURNACE   OPEN-FURNACE
              ARRANGEMENT     ARRANGEMENT
                 OPEN-FURNACE
                 ARRANGEMENT
                Figure 5-9.  Types of cyclone furnaces.
38
EMISSIONS FROM COAL, COMBUSTION

-------
  SUMMARY OF RELATED COAL-FIRING EQUIPMENT AND USE

         Since coal firing is utilized in such a wide range of equip-
  ment, a reference chart relating the various kinds of  coal-firing
  equipment to several size-range scales and then to the types of
  buildings  in which the equipment is utilized has been prepared to
  aid in emission inventory studies (see Figure 5-10).

         The classification of building occupancy and plant grouping
  is that shown in Table  5-1.


  Table 5-1.  BUILDING AND PLANT HEATING REQUIREMENTS
Group
               Building or plant category
                                                             Range of heat
                                                           input, 10*" Btu/hr
  II




  III


  IV



  V

  VI

 VII
Residential (primarily space heating).
  Residential, 1-4 family.
  Residential, multiple dwelling, large apartment.
Institutional and commercial (primarily space heating).
  Schools, churches, small colleges,  small hospitals, librar-
     ies, other public buildings.
  Office buildings, hotels, theaters, stores (core area and
     business district).
Business and manufacturing without high process steam re-
  quirements (primarily space heating).  Manufacturing,
  warehousing, wholesaling.
Large institutional and manufacturing (primarily space heating
  Large colleges, hospitals, large housing projects, or other
     institutional complex with large central boiler plant.
  Community central heating plants (utility).
Small industrial (with high process steam requirement).
  Dairies, laundries, dry cleaners, food process, etc.
Large industrial (with high process steam required or electric
  steam generating facilities). Large industrial plants.
Public utility steam electric generation station.
  0-1.0
0.5-5.0

  1-50

  1-50

  1-50



 10-200

100-500
  1-100

 10-600

 100 up
"Groups have been arbitrarily numbered for purposes of this report.
        Size ranges of boilers  are also commonly stated in pounds
  of coal per hour input and boiler output in thousands  of pounds
  of steam per hour.  In order to relate the boiler input in pounds
  of coal per hour to  10& Btu per hour, the average heating value
  of 13,100 Btu per pound for United States coal was used. * Boiler
  output was determined by applying the coal-to-steam efficiencies
  shown on Figure 5-10.  These are the  typical efficiencies found
  for the size and type of equipment indicated.

        The general relationship between combustion gas condi-
  tions of temperature and excess air for the various  sizes of
  equipment is included only as an indication  of what might be
  expected.  These relationships  are important in standardizing
  stack gases.
  How Coal is Utilized
                                                                      39

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40 EMISSIONS FROM COAL COMBUSTION
CLASSIFICATION
OF
BUILDI»C MO |
PUHT ]

FIRING METHODS
EFFLUENT
TEMPER* TU RE, °F
COAL-TO-STEAN
EFFICIENCY. <
EXCESS AIR, J
STACf
EFFLUENT? cf»
ELECTRICAL
GENERATION MX
STEW OUTPUT,
1,000 Ib/hr
COAL IKPUT. Ib/hr
HEAT INPUT
106 it u /hr,
0
|
j 1 GROUP VI i - PUBLIC UTILITY STEAM ELECTRIC GENERATION STATION
(GROUP VI - LARGE INDUSTRIAL WITH PROCESS STEAM [ ! 1
IGROUP V SHALL INDUSTRIAL WITH PROCESS STEAM DAIRIES, Etc.| | J



1 IGROUP IV8ICENTRAL PLANTS) 1 |
GROUP IV A - LAHGt INST. HOSPS, fete. | | j
GROUP MB- OFFICE BLOS. HOTELS, THEATERS. Etc, ! j
GROUP II A - SCHOOLS, CHURCHES. SH1COUEGES. Etc ; 1 [
| GROUP 1 6 - APARTMENT BUILDUPS | 1 i ! ',
GROUP IA l-to 4 FAMlDWELLINGSI 'III

! ( CHAIN or TRAVELING GRATE | | 1
| WATER COOLED VIBRATING GKATT | | [
J SPRa- TRAVELING GRATE 1 1 1
[SPP^-STATIONARY or DUMPING GRATE | GRATE 1 |
! ISPR"IVIB. GRATE| ' 1
(6CR AUTO|PACK»GED BOILER] | MULTIPLE RETORT UNDERFEED STOKER ] j 1
SINGLE RETORT UNDERFEED STOKER j _J j i J
HAND-FIRED EQUIPMENT 1 1 " j
! '" " ! ! ' 1
i i ! !
1 |
1 1 Illl II
SCO 750 700 650 ! 600 550 i 500 150 400 j 350 300
: 1 * ' i
! ! : : i
j i i i i ii i
55 60 65 ' 70 i 75 80 i 85 ',
! 1 i 1 I
! i ! !
L 1 1 III
1 1 1 1 1 1 1 1 1
100 90 85 75 70 65 60 56 50 j 15 40 35 30 ' 25
i ! : j :
,1111111 1 1 1 1 1 Illl 1 1 1 1 1 1 III 1 1 1 1 1 1 III 1 1 1 1 1 1 1 II 1 1 1 II III
50 100

500 1.000 j 5.000 10,000 j 50.000 100.000 I 500,000 1.000,000 1 5.000.000 10.000.000
1 1 1 1 1 Mill 1 I 1 1 I Mil 1 1 1 1 1 Illl 1 1 1 Mill


i JIO 50 100 500 1.000 5.000
! i i i
Mill 1 1 1 Illlll 1 1 1 1 1 Illl 1 1 Mllll 1 1 1 1 Mill 1 1 1 1 1 Illl 1 1 1 1 III
D.I 0.5

1.0 5 1 10 50 ] 100 500 jl.OOO 5.000 .10.000
1 ,' « 1
Illl
1 1 1 1 1 Mill 1 1 1 II 1 III 1 1 1 1 Mill 1 1 1 1 II III 1 1 1 1 II III 1 1 1 1 II
10 50

! 1 1 1 1 1 III
100 500 ' 1.000 5.000 ! 10. 000 50000 i 100,000 500.000 I 1.000. 000 5.000.000
i ! '
I
1 1 1 1 1 III 1 1 1 1 Mill 1 1 1 1 1 Illl 1 1 1 1 1 Illl 1 1 1 1 1 1 II
.1 0.5 1.0 5 lo 50 500 1.000 5.000 10.000 50.000


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                       CHAPTER VI.

    SMOKE EMISSIONS AND COMBUSTION PLUME


 THEORETICAL CONSIDERATIONS

      The combustion plume is a visual manifestation flowing
 from a stack or chimney,  which reduces visibility by the
 scattering or absorption of light.  The plume may result from
 the presence of submicron-size solids, liquid particles ranging
 in size from 0.01 to 2 microns with the greatest number of
 particles being approximately 0. 3  to 0. 6 micron, 34> 35
 gases that manifest visible color.
      The visible plume from the combustion of coal may be
 caused by one or all of the following:  condensed water vapor,
 sulfur trioxide, sulfuric acid,  organic liquids and gases,
 particulates, and smoke.  Water vapor condenses and produces
 a white plume, which dissipates rapidly.  Sulfur trioxide and
 sulfuric acid cause a detached bluish-white plume that does not
 dissipate readily.  Organic liquids and solids may cause a white,
 yellow, or brown plume, whereas the particulates (including fly
 ash) cause the  plume to be white, brown,  or black in  color.
      Although much has been written on the subject, the theory
of smoke formation is not well understood. As far back as 1913,
Porter and Ovitz3" explained that visible smoke consists of solid
carbon particles and solid or liquid hydrocarbon particles, or
"tar vapors, " resulting from the incomplete combustion of the
volatile products of the fuel.  The carbon of the smoke is not
derived from the free  carbon in the fuel, but result from, the
cooling of hot,  dissociated hydrocarbon gases.  Thus,  the smoke
as referred to in this report, is defined as the black portion of
the combustion plume.


      Once formed,  carbon soot is difficult to burn.  For this
reason, air supplied over the fuel bed should be admitted at or
as near the surface as possible and mixed with the hydrocarbons
so that they will burn before they are decomposed by heat into soot
and smoke. 29,37
                              41

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 PLUME EMISSION MEASUREMENT METHODS
 Ringelmann Chart

       The standard method of evaluating the severity of smoke
 plume is a visual comparison of the color shade of the plume
 with shades of gray of the Ringelmann Chart.  Other devices
 have been used, but,  in general, they are standardized against
 or related to the Ringelmann numbers.

       The Ringelmann Chart,  as described by a Bureau of Mines
 Publication, 38 establishes shades known as Ringelmann No.  1,
 2, 3>, and 4,  respectively, with No.  0 being clear and No. 5
 being 100 percent black.   Thus, No.  1 is related to 20 percent
 density; No.  2,  to 40 percent  density; and so on.

       To evaluate smoke emission over a period of time, the
 average percentage density of the smoke  for the entire period
 of observation is obtained by the formula:
Equivalent units of No.  1 Ringelmann  x 20   Average percentage
         Number of observations               smoke density.
 By the same methodology, the "average smoke density" of a
 large number  of combustion sources over a time period can be
 determined.
 Equivalent Opacity

       The evaluation of a plume of any color may be accomplished
 by comparing the opacity of the plume to an equivalent shade of
 gray on the Ringelmann Chart. ' '  This method evaluates not only
 smoke but also non-settling particulates, sulfur  trioxide,  etc.
 The evaluation  is reported in terms of percentage of plume
 opacity and can be calculated in a manner similar to that of the
 smoke calculations for average density.


 Soiling Potential

       A procedure of drawing a measured volume of air through
 a white filter paper tape and evaluating the resultant stain;by
 optical means has been used for many years as an index for
 atmospheric pollution buildup.  It was first applied by Hemeon
 in  1953 to evaluate the severity of smoke emission from a

 42                      EMISSIONS FROM COAL COMBUSTION

                                                       GPO 825-629-^*

-------
power plant chimney. 4" Since that time, the continuing measure-
ment of soiling index has been used by many communities as one
of the basic, outdoor air quality appraisals. 41, 42  This method,
however,  has not been used extensively as  a means of quanti-
tating smoke emissions  from the combustion of fuels  until
recently. 42  The procedure is similar to that recommended by
the Air Pollution Control Association for ambient air measure-
ments. 43   The quantity of  emissions  are reported as  Coh-ft^
per pound of coal when evaluation is  by light transmittance  and
as Rud-ft  per pound of coal, when evaluation is by light reflect-
ance.  The advantage of this method  over those mentioned earlier,
is that it provides data that can be inventoried from all sources
and compared with conventional  atmospheric measurement
(soiling index).

Smoke Spot Tester

      For a number of years , the smoke spot method of testing
smoke density in the flue gases from distillate fuel oils has been
used with success to evaluate oil burner performance,  particu-
larly of smaller units.   This procedure is described as a pro-
posed method, published by Committee D-2 of the American
Society for Testing Materials. 44 Although the method produces
a relative value of the soiling potential, it has not been extended
to quantitating emissions.

      The Air Pollution Control  Division of the Department of
Works,  Metropolitan Toronto, evaluates combustion equipment
fired by all fuels, oil, gas, and  coal, with  the Bachrach Smoke
Tester, which conforms with the American Society for  Testing
Materials method.
PLUME EMISSION DATA

Smoke in Average Percent Density

      Values of average percent smoke density for a large number
of units .operating in a given community are difficult to find.  One
such project was conducted in the City of Cincinnati in 1939-
1940. 45  Smoke emission readings in Ringelmann numbers were
taken from vantage points throughout the entire city.  The number
of operating  chimneys, mainly residential units,  were known,
and the smoke readings  in Ringelmann numbers were compiled
into average percentage density values as shown  in Table 6-1.

      In  1939, Cross, et al. ,    conducted a field survey of 22
small stoker-fired boiler plants and found the average Ringel-
mann Number to be 0. 5 with the stokers on and 1. 0 with the

Smoke Emissions and Combustion Plume                     43

-------
         Table 6-1.  AVERAGE PERCENTAGE SMOKE
           DENSITY FROM OPERATING CHIMNEYS,
               CITY OF CINCINNATI, 1939-1940
       All chimneys (except basin area)
       Basin area only
       Coal-fired railroads
       River boats only
                                        Smoke density, %
                     7.8
                    21.0
                    28.0
                    23.7
 stokers off.  Corresponding percentage of smoke density are
 10 and 20 percent,  which were explained earlier.
       It would be expected that improvement in stoker-firing
 equipment has reduced the average percentage smoke density
 for a given population of small stoker-fired plants to approx-
 imately 10 percent average smoke density or one-half Ringel-
 mann average.
       Estimated average percentage smoke densities for 24-
 hour operation,  based on the above information, are shown in
 Table 6-2.
 Table 6-2.  ESTIMATED AVERAGE SMOKE EMISSION FROM
                SMALL STOKER-FIRED PLANTS
Where good air pollution controls are exercised
Where average operation is experienced
Where poor operation is experienced
                                                  Average
                                              smoke density, %
                            10
                            20
                            40
 Plume Equivalent Opacity
       There is very little published work evaluating equivalent
 opacity of the combustion plume, although most smoke recorders,
 44
EMISSIONS FROM COAL COMBUSTION

-------
mounted in the boiler stacks, record the light transmission or
opacity of the whole plume, not just black smoke.  In 1963,
Haugebrauck, et al. , 47 measured total particulate ( after the con-
trol equipment) and, incidentally, noted the equivalent opacity of
the plume ( Table 6-3).  As shown by the data of Table 6-3, no
direct relationship seems to exist between the total particulate
loading and the  opacity of the smoke plume.
       Table 6-3.  PLUME OPACITIES FROM VARIOUS

                  TYPES OF EQUIPMENT47
Firing method
1. Pulverized
2. Pulverized
3. Chain- grate stoker
4. Spreader stoker
5. Underfeed stoker
6. Underfeed stoker
7. Underfeed stoker
8. Hand -fired
Total particulate,
pounds per 10 Btu
'0. 59
2.23
1.31
0.82
0.62
0.25
0.44
1.29
Plume opacity,
percent
30-40
60
20-40
0-20
20-40
0-20
0-20
40-80
Soiling Potential

      Data from 17 tests by the Division of Air Pollution Control,
City of Cincinnati,42 showed an average value of 134 Rud-ft2 per
pound of coal burned; the measured values ranged from 9 to 1,250
Rud-ft2 per pound of coal burned.  Results from these tests indi-
cated that good combustion should yield values of less than lOORud-flr
per pound of coal, whereas poor operation would be well above
1, 000 Rud-ft2 per pound of coal.

Smoke Spot Data

      In 1939, the Bureau of Air Pollution Control,  City of
Cincinnati, applied the smoke spot method to smoke performance
tests of various coals fired in a small space heater (not published).
Bachrach smoke spots were taken every 4 minutes for 1 hour after
a uniform  charge of coal was fired by hand upon an established
 Smoke Emissions and Combustion Plume
45

-------
fire bed.  Figure 6-1 shows the  1-hour average values of smoke
spot numbers versus percent volatile matter in the coal.

Mass Emission and Smoke Plume

      In this country, little interest has been shown in relating
the severity of the plume to mass emission units.  Many authors
have pointed out quite explicitly that most smoke plumes contain
only infinitesimal weights of particulate matter,  even though at
times black smoke produced .by the incomplete burning of hydro-
carbons may seem so dense as to appear to be solid black.  The
opacity is  due to the presence in the plume of a tremendous num-
ber of small particles in the size range of 0. 3 to 0. 6 microns,
which have a highly effective light absorbing or scattering effect,
     0     1
      Figure 6-1.
 23456     789
  AVERAGE BACHRACH SMOKE NUMBER
       (ONE STROKE OF PUMP)
Relative soilinq potential of various coals as  related
      to their volatile content. ^
 46
                          EMISSIONS FROM COAL, COMBUSTION

-------
but contribute little to the mass of the emission in relation to the
larger particulates in the plume.  The mass of the  emission is
contributed by the larger particles,  which may have little  light
absorbing or scattering effects.
                                   40
      Some of the work done is of interest, however.  One author
related total loading to percent of light absorption for a stoker-
fired,  warm-air furnace, burning approximately 20 pounds of coal
per hour and determined particulate sizes to be  mostly 1 micron
or less (Figure 6-2). 48
   2.4
               o > 900
               A 700-900
               0500-700
                 <500
      0     10     20    30    40     50     60     70    80    90
              "TOTAL  LOADING" AT 60 °F. grains/ft3
      Figure 6-2.  Relationship  between "total"  particulate emission
                       and light absorption.^8
      In England, Hurley and co-workers4*?, 52 investigated the
relationship between mass emission rates and opacity on hand-
fired and small stoker equipment (Figure 6-3).  Of greater in-
terest than total emission is the composition of the particulate
( Figure 6-4), which shows a marked rise in both carbon  (soot)
and tar (benzene soluble) as smoke density increases.  This
rapid rise in the tar content as smoke increases is a most im-
portant consideration in assessing the overall effect of the
"visible smoke" plume upon the community.
Smoke Emissions and Combustion Plume
                                                             47

-------
             0
              6   8   10   12  14
                   SMOKE NUMBER
                                           6   18  20   22


Figure 6-3.  Relationship between solids emission and opacity.^
         s? -
60.

50

40

30

20

10
                    ASH
                                    s^hK
                                           7
                                     HYDROGEN
                                          I
12

10 ^

 8 £
   Q
 6 i

 4|
   o:
 o o
              8   10  12  14  16  18  20  22
               SMOKE NUMBER
           0   2  4   6

  Figure 6-M-.  Relationship between  pollutant, emissions and smoke opacity.1*9
REDUCING SMOKE EMISSIONS

      Techniques for reducing smoke formation from the burning
of coal are very well understood and are generally applied, par-
ticularly in areas having air pollution control programs.  The un-
bridled ^mission-of black smoke from home and industry chimneys
motivated smoke control programs in many communities at the
turn of the 19th century.
 48
              EMISSIONS FROM COAL COMBUSTION

-------
Hand Firing

      The only practical method of controlling excessive smoke
from hand-fired furnaces is to use a coal of relatively low vola-
tile content, varying from 26 percent down to 20 percent or less
on a moisture-  and ash-free basis, depending upon the degree of
control desired.  Good firing practices, assisted by well-designed,
over-fire air jets, are partially effective in some larger furnaces
when trained firemen are used, but such installations are fast
disappearing, being replaced with automatic firing.


Small Underfeed Stokers

      The construction of a smokeless installation requires attention
to numerous details, which can be grouped into five general guides.

      1. The firebox dimensions, .including combustion volume,
         flame clearance, and burning rates, should meet the
         standards contained in the "Technical Manual on Single-
         Retort Underfeed Stokers" published by the Air Pollution
         Control Association.  3

      2. Stoker controls should match the load requirements; and
         for units consuming more than 800 pounds per hour, step
         control for the coal feed rate and combustion air should
         be provided.  Automatic furnace draft control is  also
         essential.

      3. Over-fire air systems are beneficial on all stokers and,
         in particular, on those with on-off control.  Design should
         comply with the recommendations developed by Bituminous
         Coal Research. 54

      4. An electric smoke-indicating and/or alarm system can be
         of assistance to the boiler operator.

      5. Adequately sized chimneys for draft are necessary, as well
         as adequate air openings, to  supply combustion air to the
         boiler room.
Large Boiler-Firing Equipment

      As the size of boiler and firing equipment increases,  the
inherent premium for  complete combustion and smokeless
operation is greater.  As a result, less control need be exer-
cised by the control official over the dimensional specifications
Smoke Emissions and Combustion Plume                     49

-------
of the combustion unit.  Larger units are generally well de-
signed by experienced engineers striving for the maximum Btu
recovery, the end result being  a relatively smoke-free plant.
This same motivation does not  usually transfer to the selection
of fly-ash-prevention equipment.   In this regard, much influ-
ence is exercised by the local air pollution control regulation.

      Heretofore, the degree of control over the smoke fraction
of the particulate emission was judged solely by a reduction in
the visible emission.  Utilizing soiling potential (expressed as
either Rud-ft2 or Coh-ft2 per 10^ Btu input), the factors con-
tributing to soiling or haze-producing effects in the atmosphere
can be determined more precisely, resulting in improvement
in the effectiveness  of control methods.
50                      EMISSIONS FROM COAL COMBUSTION

-------
                     CHAPTER  VII.
           PARTICULATE EMISSIONS
THEORETICAL CONSIDERATIONS

      The emission of solid matter from a given furnace is
related to many factors, mainly gas velocity, particle size,
particle density, fuel-burning rate,  combustion efficiency, flue
gas temperature,  furnace configuration, coal composition and
size, and the initial state of the raw coal.  An indication of how
these variables  affect the emission rate is shown in Table 7-1.

      For any specific furnace, the composition of the fuel is the
largest variable.  The primary consideration in burning a fuel
is to maximize heat release while minimizing costs.  This does
not always mean 100 percent combustion.  As noted in chapter IV,
         Table 7-1.  SOME VARIABLES AFFECTING
              PARTICULATE EMISSION RATES
Variable increasing
Gas velocity
Particle size
Particle density
Coal ash
Coal size
Coal fired in suspension
Coal -burning rate
Coal heat value
Combustion efficiency
Boiler efficiency
Mass particulate rate
Increasing
X


X

X
X



Decreasing

X
X

X


X
X
X
                              51

-------
the optimum efficiency is usually about 95 to 99. 5 percent of
complete combustion. 31  Ideally, the only particulate emission
would be the mineral ash contained in the coal; however,  0. 5 to
5 percent of the combustible content of the coal can also be
emitted as par ticulate matter.  (There cannot be more than
100 percent of the ash in the coal emitted as noncombustible
matter.)  Thus, more particulate matter can be emitted than
there is  ash in the coal because of the combustible fraction in
the emissions.  If reinjection of fly ash is practiced, there can
be an accumulation in the furnace of suspended solids repre-
senting more than 100 percent of the ash in the fuel and, thus, a
factor representing the solids  leaving the furnace (before the
fly-ash collector) can be greater than the total ash entering in
the fuel;  however, when the collector is included in the emission
calculations,  this is not true.

      As the velocity of the gases passing through the furnace
increases, larger particles of coal and ash are carried out of
the furnace.   The velocity of the gases is directly proportional
to the firing rate of a given furnace; thus the size of the particle
and rate of emission should be  a function of the firing rate.  In
a similar manner, the excess  air, pressure, and temperature
are related to the particulate emissions in that they control the
gas velocity.

      The method of burning the coal also influences  particulate
emission rates.  When coal is thrown or blown into a furnace,
combustion takes place in suspension. As the pieces of coal
burn, they get smaller,  and thus their chance of being  exhausted
•with stack gases is increased.  When coal is pushed or pulled
into a furnace, to form a bed,  the coal or ash has less chance of
being entiained by the flue gases because of impingement onto
larger particles.  When coal is introduced tangentially into a
cylinder, such as in the  cyclone furnace, the burner acts as  a
cyclone separator and thus reduces emission of larger particles.

      If all of the variables were known,  the amount of particu-
lates  emitted from a given unit could be predicted.  The problem
is that none of the above variables are completely known.  The
following variables are felt to be the most important in relation
to particulate emissions:

      1.  Amount of ash in the coal.
      2.  Heat content or heating value of the coal.

      3.  Method of burning the coal.

      4.  Rate at which the coal is burned.

 52                      EMISSIONS FROM COAL, COMBUSTION

-------
      Hand-fired equipment is treated separately from mechan-
ically fired furnaces because of the difficulties in obtaining,
representing, and interpreting the data.
EMISSION UNITS

      A wide variety of units have been used by various authors
for reporting emission rates,  such as  a percentage of the ash
in the coal, a percentage of the coal burned, pounds per  10° Btu
input,  grains per cubic foot of stack gas,  and pounds per thousand
pounds of flue gas.  Some authors have reported  the conditions
at which their units are  standardized,  such as the temperature,
percent carbon dioxide or excess air,  or  type of  coal, whereas
others have assumed that conditions considered "standard" are
understood.

      In the selection of emission units for this report, primary
consideration was given to the effect that variation in the com-
position of coal has on emission rates.  Consideration was  also
given to the principal usage of the coal, namely to produce  heat.
In an attempt to combine these two facets  into one factor, several
correlations were developed.  The heat content (on a dry basis)
was  plotted against the ash content (on a dry basis) for coals
from the individual producing districts of the country (Figure 3-2,
chapter III), and the nomograph in Figure 7-1 was developed to
show this general relationship.


      Because of the many  different units  used in reporting emis-
sion data,  utilizing conversion factors  from standard handbooks
was  convenient to produce a series  of nomographs to assist in
converting units  and making elementary combustion calcula-
tions.   ' 12,31,55 pertinent relationships developed are given
in Figures 7-2 and 7-3.

      With these relationships, one can see that the composition
of the fuel is related to the stack gas concentrations only through
the heat content of the coal. Thus,  since  the composition of the
fuel  is so highly  variable,  the emissions  should be stated in
terms  related to composition,  i. e. ,  pounds of pollutant per
10° Btu input.  An estimate of particulate emissions, therefore,
requires knowledge of the ash content and heating value of the
coal, type and size of the combustion unit, and control equip-
ment efficiency.  With this  knowledge,  an estimate may be  made
of the mass rate of emission of particulate pollutants per unit
time or stack concentrations of particulate from various units
with and without various types  of control equipment.

Particulate Emissions                                       53

-------
 ASH CONTENT,

    20-i


    18-


    16-


    14-


    12->v
         \

    10-


    8-


    6-


    4-


    2-


    0-
                           HEATING  VALUE,
                             Btu/lb
                            r 16.000
  H»
 G»
'S.
  F«
  E»
  O
  B»
     A«
             - 15,000
             - 14.000
-13.000
             - 12,000
             - 11 ,000
                            L 1 0.000
           POINT

             A
             B
             C
             D
             E
             F
             G
             H
  PRODUCING
  DISTRICTS

     21
     19
     16
    17,22
     12
4,9,10.11
   3,6,15
    2,8
  1,13,14
     7
18,20
 ANTHRACITE
  Figure 7-1.  Relationship between ash content and heatinq value for coals
                  from various producing districts.
PHYSICAL PROPERTIES OF PARTICULATES


Particle Size Distribution

      Many authors have reported particle size distributions for
various types of equipment.  Most of these distributions were
termed "typical, " although a few were based on specific stack
test data.  Some authors reported other data with the size
analysis, such  as  combustible content or firing rate.  Some data
represented the size analysis of dust taken from a collector or
precipitator, whereas other data represented  size distributions
54
         EMISSIONS FROM COAL COMBUSTION

-------
of dust passing uncollected through control equipment.  Figures
7-4 through 7-7 present only those data believed to represent
the size of the particles leaving the boiler or furnace before
any control equipment.  Attempts were made to separate the
data, according to broad types of combustion equipment.  The
data were equally scattered for all types of stokers other than
spreader stokers  and were therefore combined into one grouping.
   100-


    90-


    80


    70-


 *«•  60-
 oT
 
-------
                  100 T
I
K
Cfl
cn
i
n
o
o
cn
8
o:

<
                   80-
                   70-
    60-
                   50-
                   to-
    30-
                   20-
                                                                                 - METHANE


                                                                                 - AVERAGE NATURAL GAS


                                                                                 -ETHANE

                                                                                 -PROPANE

                                                                                 - BUTANE

                                                                                 -PENTANE

                                                                              60.. 'GASOLINE
                                                                                             '*5- -
    > MEDIUM VOLATILE
    '  BITUMINOUS
                                                                                   .SUBBITUMINOUS
                                                                                    AND LIGNITE
                                 Figure 7-3.
 HIGH  VOLATILE
  BITUMINOUS

 LOW VOLATILE
  BITUMINOUS  '

SEMIANTHRACIT


  ANTHRACITE-



         COKE-
                               Relationship  between type of fuel burned and excess air,  and
                               resulting percent oxygen and carbon dioxide in flue gases
                                            (adapted from reference 55).
                                                                                                  KEROSENE
35- - No. 2 FUEL OIL
25-- No. 4 FUEL OIL


15- - No. 5 FUEL OIL
10-- No . 6 FUEL OIL
                                                                               5~ > BUNKER
                                                                               2-J
                                                                                                          'C" OIL
                                                                                                            v
                                                                                                            I \

-------
No difference was found between wet- or dry-bottom pulverized-
fuel-fired furnaces; therefore, in Figures 7-4 through 7-7,  the
size analysis ranges (dashed lines) and a typical analysis were
chosen by the authors to represent the very scattered data.
   10
    O.Ot  0.050.10.2 05 I  2   5  10   20 30 40  50  60  70  00   90  95  96 99   99.090.9  99.99
                     PERCENT BY 1EIGHT LESS THAN STATED PARTICLE SIZE

Figure 7-M-.  Estimated size distribution for particles emitted  from pulverized-
               fuel-fired furnaces  (before collectors).

      One important variable was  found with  respect to the
pulverized-fuel-fired units.  Some of the data°2,85  revealed
that one could expect larger particles when the combustible
content was high and smaller particles when  the combustible
content was low.  This is only a generalization, and numbers
cannot  be assigned  to various size analyses because this relation-
ship varied so much between units.  This relationship may be
true of other types  of units also, but because of a lack of data
with supporting operating information,  no definite conclusions
can be  drawn.  It might be  expected that the particle size -would
increase with an increase in firing rate or  exhibit differences
with the use or nonuse of fly-ash reinjection; however, no such
correlations were found.
 Participate Emissions                                        57

-------
    20
    10
     0.01
         I  I  I	1—I	T
          CURVES 3ASEO ON DATA IN
          REFERENCES 96 through 52
                                  ~\	1—I	1	T
                                                                -T—r
                                                            RANGE REPORTED
         I  I  I	I_J	L
                        J	L
                                I   I  I	L
                                                         i	L
                                                                 I  I
         0.090.1 0.2 0.5
                        5  10   20  30 «  50 60  70  80  90
                       PERCENT BY HEIGHT LESS THAN STATED PARTICLE SIZE
                                                         96  99
                                                                98.B 99.0  96.99
 Figure 7-5.   Estimated size distributions  for particles  emitted from cyclone
                        furnaces (before collectors).

Particle Description

       Microscopic  analysis  of fly ash,  using reflected light, will
indicate the type of firing unit that was the  source as well as the
combustion efficiency (Table 7-2).   Additional information can
be found in reference 86.
            Table 7-2.  CHANGING VARIABLES WITH
                    MICROSCOPIC ANALYSIS
                                                 62
Type of unit
Pulverized units
Spreader stoker
Other stokers
Domestic units

Small particles
i

Large particles
Glassy and
spherical


Flaky and
agglomerated
Low carbon
i
I
High carbon
  58
EMISSIONS FROM COAL COMBUSTION

                                 GPO 625-629-5

-------
   100
          ~r~i  i  I   i   I   i	1—i—i—i—i—i—i	1	1	1—i	r~r
          CURVES BASED ON DATA IN
          REFERENCES 58. 59. 66.
          and 71-77.
                                         RANGE REPORTED
         	/ // I   I	|	I	I	|	|	L.	I	I	I
    10
     0.01  0.050.1 0.2 0.5 1  2   5  10   20 30 40  50 60 70  80  90  95   98  99   99.B 99.9 99.99
                     PERCENT BY iEIGHT LESS THAN STATED PARTICLE SIZE

 Figure 7-6.  Estimated  size distribution for particles emitted  from spreader-
                stoker-fired  furnaces (before collectors).

Particle Density

      The density of fly ash depends primarily on its particle
size, particle structure, and carbon content. 56, 87 ln general,
the large, coarse particles, containing a high percentage of
carbon, have a low density.  It appears that the volatile portion
burns out, leaving black,  coke-like particles, having low densi-
ties and a specific gravity on the order of 0. 6 to  1. 0. ", 87  One
investigator^  reports a specific gravity of 0. 7 as  compared to
the average  value for  fly ash of 2. 0 to Z. 7. 57, 89  in evaluating
the importance of the  physical and chemical properties of fly ash
for commercial use, values of 2. 28°° and 2. 0°"> '3 for  specific
gravity have been reported.

      Finer  particles  of ash, which tend to be low in carbon
content have a much higher specific gravity, usually in the range
of 1. 5 to 3. 56, 59, 88  -phe very small particles may run well
over 4. 0^9. 88 an(j ,jo not exhibit the porous  structure  of the
larger  particles, although many of them may be hollow spheres
or cenospheres.

Particulate Emissions                                         59

-------
         CURVES BASED OH DATA IN
         REFERENCES II. 19 57-59
         62-66. and 71-84.
                                                         M.8 H.t H.99
                    PERCENT BY IEIQHT LESS THAN STATED PARTICLE SIZE
 Figure 7-7.  Estimated size distributions for particles emitted from stoker-
         fired (other than spreaders),  furnaces (before collectors).
      The variation in density with particle size for typical fly
ash from a modern pulverized-fuel-fired boiler is shown in
Table 7-3.  Also given are the corresponding bulk densities of
the size fractions.  The bulk density of fly ash usually ranges
from 30 to  50 pounds per cubic foot^k, 88 but may be as high as
90 pounds per cubic foot. ^°  Freshly collected, hot  fly ash is
normally very fluid and has a somewhat lower density than cold
fly ash.  The fresh fly ash is probably aerated by the exposure
of the individual particles to the carrier gas, which results  in
adsorption  of gas layers on the particle surface. De-aeration
of the ash tends to occur after standing and cooling, which cause
the ash to compact and become less fluid. ^6  One author reports
that the bulk density of freshly precipitated fly ash may be as
low as  15 pounds per cubic foot, but upon standing and complete
removal of occluded gases, the ash may have  an increased
density of 40 to  60 pounds per cubic foot. 91

CHEMICAL COMPOSITION OF PARTICULATES
      Chemical compositions of particulate emissions are as
variable as emission rates.  The inorganic portions vary with

60                       EMISSIONS FROM COAL COMBUSTION

-------
the ash analysis of the coal (see chapter III).  Tables 7-4 and
7-5 show representative data found in the literature.  These
analyses show that the major constituents of most fly ashes
  Table 7-3.  DENSITIES OF PARTICLE-SIZE FRACTIONS
      FOR A TYPICAL PULVERIZED-COAL FLY ASH
                                                      56
Particle-size
fraction, microns
Total sample
< 44
44 to 74
74 to 149
149 to 297
>297
Percent present
100
78
10
8.3
3.6
0. 1
Density,
g/cm3
1.75
1.78
1.70
1.60
1.57
1.02
Bulk density,
g/cm3
0.58
0.60
0.44
0.38
0.25
0.21
lb/ft3
36
37
27
24
16
13
       Table 7-4.  RANGES IN ANALYSIS OF FLY ASH
Compound
Carbon, C
Iron, Fe,O, or Fe,C3
23 34
M-agnesium, MgO
Calcium, CaO
Aluminum, Al O,
2 3
Sulfur. SO
Titanium, TiO,
2
Carbonate, CO
Silicon, SiO,
2
Phosphorus, P2°c
Potassium, K O
Sodium, Na O
Undetermined
Reference
Percentage of fly ash
0.37-36.2
2.0 -26. 8

0. 06- 4. 77
0. 12-14.73
9.81-58.4

0. 12-24. 33
0. 50- 2.8

0.05- 2.6
17.3 -63.6

0.07-47.2


0.08-18.9
56
0. 56-31. 56a
3.86-26.43

0.55- 1.91b
1.00-10. 59
15. 12-34. 04

0.23- 3. 59°



28. 1 -51.26

1



92
1.4-13.5a
6. 1- 9.0

1. 3- 2. 0
2.6- 4. 3
26. 7-28.5





45.2-46. 9


2.8- 3.0
0.2- 0. 9

93
1.49-19. 51a
6. 62-26. 43

0.55- 1.63
0. 99- 9. 68
17. 50-30. 39

0.23- 3.59



34.01-47.54





94
"Ignition loss.
 Usual range, extreme range: trace - 3.0%.
cUsual range, extreme: as high as 12%.
Particulate Emissions
61

-------
are silica, alumina, and iron oxide.  The first two are present
primarily as silicates, which give fly-ash particles their typical,
glassy appearance.  Iron oxide may be present as Fe2O3, which
in appreciable amounts imparts a tan or reddish color to fly ash.
The presence of iron as magnetite, Fe3
-------
COMBUSTIBLE CONTENT OF PARTICULATES
      The combustible content has a direct relationship to the
mass emission rates and,  therefore,  is treated separately
from other chemical properties of fly ash.  The combustible
contents of fly ash from various types of units were compiled
and separated in an attempt to determine what might be con-
sidered average or typical values (see Figures 7-8 through
7-10).  Only three values were found for the cyclone unit
(14.2 and  11. 1 percent, 95 an
-------
 reason, the value of 10 percent combustible is believed to better
 represent the values for pulverized and cyclone  units.  Figure 7-9
 shows the values found for spreader stokers.  Here the most
 common value,  about 50 percent, appears to be  representative
 of spreader stokers (with or without fly-ash reinjection).
          1C
         o

         o
                                     NUMBERS IN BLOCKS ARE
                                     REFERENCES CITED
                                   RVALUE CHOSEN
N

71
71
71
66
101
oq
82
91
1

                                  "•
            0   10   20   30   40   50   60   70  80   90  100
                       COMBUSTIBLES IN  PARTI CULATES, %
       Figure 7-9.  Combustible content of particulates from  spreader-
                        stoker-fired furnaces.
      Figure 7-10 shows the values found for other types of
stokers.   The data for each stoker category were so meager
and scattered that all stoker data were combined.  In this case,
the authors chose 40 percent combustible matter as a repre-
sentative value for stokers other than spreader stokers.

a
-i
Q
1s-
U-
o
o





NUMBERS IN BLOCKS ARE
REFERENCES CITED


* VALUE CHOSEN
81 81 OC
6S| 95 80 80 95J67 67 1 4
66J , , 102, 17
67
67 95
103 67|67| |67|67| ,
                10   20   30   40   50   60   70   80   90  100

                      COMBUSTIBLES  IN PARTICULATES,  %
       Figure 7-10.  Combustible content of particulates from stoker-fired
                   furnaces (except spreader stokers).
64
EMISSIONS FROM COAL, COMBUSTION

-------
         The values for the combustible content of particulate
   matter are extremely scattered because of many variables,
   the most important of which is probably the firing rate.
   Figures 7-11 and 7-12 show correlations between firing rate
   and load,  with combustible content of the fly ash reported by two
   authors.  The actual values may not apply to the average unit
   operating today, but the relative increase could be representative.
   One author attempted to correlate the carbon content of ash to
   particle size (Figure 7-13). ^6
 100
z 60
8
UJ
f 40
S20
                            I      I	I	I	I
                0.2         0.4         0.6        0.8         1-0

                           LOAD,  I06 Btu/ft2   hr
        Figure 7-11.  Combustible content of particulates versus load fora
                     multiple-retort underfeed stoker.67
         Associated with the combustible content are the poly-
   nuclear hydrocarbons.  There is much interest in these sub-
   stances because of their carcinogenic properties.  Concentra-
   tions of polynuclear hydrocarbons in particulate emis sions
   found in the literature are shown in Tables 7-6 and 7-7.  There
   was little,  if any,  reduction in the polynuclear hydrocarbons
   after the effluent passed through control equipment.   This seems
   to indicate  that polynuclear hydrocarbons are  found in particles
   of less than 1 micron and are not easily collected. 47> 104> 105, 106
   MASS EMISSION FACTORS

          The literature contains vast amounts of data for stack gas
   particulate concentrations.  The majority of these data have

   Particulate Emissions                                       65

-------
   50






^ 40


I—~

UJ

£ 30

S

LU


= 20

GO
z>
ca
S
o

0  10
                    25
                                  I
                                                I
                                  50           75


                                    PERCENT LOAD
                            100'
125
         Figure 7-12.   Combustible content of particulates versus load for a

                       slag-tap pul veri zed-coal-fi red unit.96
                         50
                         •HO
                         30
                       Al
                         20
                          10
                                i    i    i    i    i
                            0   5   10  15  20  25  30   35

                                   CARBON IN  ASH, %




                        Figure 7-13.   Relationship between

                        ash particle  size and carbon content

                        of fly ash  from pulverized units.56
    66
EMISSIONS FROM COAL COMBUSTION

-------
 Table 7-6.
          FROM STOKER AND HAND-FIRED UNITS
SOME POLYNUCLEAR HYDROCARBONS EMITTED
                                       47
            (Values expressed in lb/10   Btu input)
Compound
Benzo(a)pyrene
Pyrene
Benzo(e)pyrene
Perylene
Benzo(ghi)perylene
Anthanthrene
Coronene
Anthracene
Phenanthrene
Fluor anthene
Benz(a)anthracene
Type of unit
Chain-grate
stoker
0.082
0.860
0.290






1. 50

Spreader
stoker
0.057
1. 30
0.770



0. 057


0.790

Underfeed
stoker
22
35
17
3.5
9.9
0. 64
0.73
1.9
22
83. 9
8. 6
0.26
3.70
0. 510





2.2
7. 1

8. 4
17
11.9

1.28

2.64

64
103
1.23
Hand-
fired
880
1,320
220
132
660
198
66
880
2,200
2,200

aA blank indicates that the compound was not detected.
little value for the purpose of establishing emission inventory
factors.  Particulate emissions are mainly a function of
(1) the ash content of the coal,  (2) the heating value of the fuel,
(3) the method by which the coal is burned, and  (4) the rate at
which the coal is burned.  If an author who reports the particu-
late emissions in the form of a concentration does not  report
the ash and heating content,  and the method and rate of com-
bustion, the values are not useful in estimating emissions from
similar coal-burning units.
      Authors also have neglected to include information about
control equipment through which the flue gas has passed before
the sample was taken.  Such an omission,  along with the others
previously mentioned, has caused much concern.  An attempt
was made to use dust concentrations reported in the literature;
but since companion data were often lacking, the dust concentra-
tion values were of little value.  The data used were principally
those expressing the emission as a fraction of the ash introduced
to the unit.   The amount of combustible material was added before
a representative value could be  ascertained.   In a previous
Particulate Emissions
                                                67

-------
 Table 7-7.  SOME POLYiSTUCLEAR HYDROCARBONS EMITTED
                                                    104
         FROM VARIOUS SUSPENSION-FIRED UNITS
             (Values expressed in Ib/10   Btu input)
Compound
Fluoranthcne
Pyrene
nenzo(a)pyrene
Bcnzo(e)pyrene
Benzo(j(hi)perylene
Corone.no
Pcrylem;
Type of Firing
Pulverized fuel
Vertical
0. 44
o. •»•;
0.04




Corner
0. 8S
0. 31
0. 11
0. 19
o. •»»
o. 02
0. IS
Front-wall
0. 18
0. 40
0.04
0. OS
0.02


Horizontally
opposed
0.41
0.20
0. 18
0. 18
1.42
0. 12

Spreader
stoker
0. 11
0.25
0.04
0. 11

0.02

Cyclone
0. 17
2.2S
0.49
(I. 87
0.44
0.01
0.04
section of this report, the percentage of combustibles for dif-
ferent units was estimated.  These values were used in this
section when reported emissions indicate that the  reported
number refers only to the noncombustible portion of the particu-
late emission.  (Example: in a hypothetical case,  40 percent
of the ash is slagged  in a wet-bottom pulverized-fuel-fired unit
and, therefore,  60 percent of the ash is emitted from the stack.
From a previous section of this report, a value of 10 percent
combustible was  estimated for particulate emissions from
pulverized firing.  This would mean that the 60 percent ash
value represents only 90 percent of the total emission, and the
total emission expressed as  a percentage  of the ash would be
60/0. 9 or 66. 7 percent.)

      In this report,  all ash fractions represent the total particu-
late emission (ash and combustible  content) expressed as a
percentage  of the ash in the  as-fired coal.  The values are
assumed to represent the emissions leaving the boiler before
any control equipment but include emissions from soot blowing.
(Cinder catchers in the boiler are assumed to be part of the
combustion unit and not control equipment.)  If fly-ash reinjec-
tion is practiced, the emission value  may exceed 100 percent
because of recirculation and accumulation of the fly ash within
the boiler passages.   It must be understood,  however, that in
order  to recirculate  the fly ash, some of it must be collected.
This means that  any  unit utilizing fly-ash reinjection must have
a fly-ash collector.
 68
                        EMISSIONS FROM COAL COMBUSTION

-------
      Figures  7-14 through 7-19 show the total particulate
values found for various units expressed as a percentage of the
ash in the as-fired coal.  Several values were given for pul-
verized-fuel-fired units in general (Figure 7-14).  The most
common value centered around  80 percent.  Figure 7-15 illus-
trates values found for  dry-bottom pulverized-fuel-fired units,
with 85 percent selected as the  most representative value.  Fly
ash is often reinjected into wet-bottom pulverized-fuel-fired
units and,  therefore, it must be represented by two values
(Figure 7-16).  Values  chosen are 65 percent for units without
reinjection and 120 percent with reinjection.  For the cyclone
unit (Figure 7-17), 10 percent was chosen as  a representative
number.  Operation of spreader stokers, like wet-bottom
pulverized-fuel-fired units,  often utilizes fly-ash reinjection.
Useful data found for spreader  stokers are shown in Figure 7-18.
Values chosen to represent these data are 65  percent for spreader
stokers without fly-ash reinjection and 100 percent for those with
reinjection.  Values for other stokers, such as underfeed,  chain -
or vibrating-grate stokers,  of all sizes are shown in  Figure 7-19.
       15-
           A VALUE OF 10% COMBUSTIBLE MATTER
           WAS ADDED WHEN AN AUTHOR INDICATED
           HIS VALUES REPRESENTED ONLY ASH EMISSION.
           NUMBERS IN BLOCKS ARE
           REFERENCES CITED
                                    * VALUE CHOSEN







108
95|l09|62|6l]
62
62
62
62
62
07



69
60
107



80 |l07|

         20  30    40   50   60   70   80   90   100   110   120
               TOTAL PARTICULATES AS PERCENT OF ASH IN COAL
       Figure 7—14.  Particulate emissions from pulverized-coal-f i red
                         units (qeneral ).
 Particulate Emissions
                                                              69

-------



CO
S'O-
«*
>•
s
en
o
0-
LU
:»-
o
0
A VALUE OF 10% COMBUSTIBLE MATTER
WAS ADDED WHEN AN AUTHOR INDICATED
HIS VALUES REPRESENTED ONLY ASH EMISSION.


NUMBERS IN BLOCKS ARE
REFERENCES CITED

•¥• VALUE CHOSEN

104
1(M 66
105 106 62
104
62
113
58

95 95 62

111
112110
70 1 14 97
58 95
23 63 62 62 |62|62] |62| 62
            50    60    70    80   90    100   110   120   130   140   150
                TOTAL PARTICULATES AS  PERCENT OF ASH IN COAL  BURNED

     Figure 7-15.  Total  particulate emissions from  dry-bottom pulverized-
                                  coal—fi red units.
                                                  A VALUE OF 10% COMBUSTIBLE MATTER WAS
                                                  ADDED WHEN AN AUTHOR INDICATED HIS
                                                  VALUES REPRESENTED ONLY ASH EMISSION.
             30   40   50   60   70    60   90   100    110  120   130 140   150  160  170
                 TOTAL PARTICULATES AS PERCENT OF ASH IN COAL  BURNED
     Figure 7-16.   Particulate emissions  from wet-bottom, pul veri zed-coal-
                                    fi red  units.
70
                               EMISSIONS FROM COAL COMBUSTION

-------
o
i
en
i

A VALUE
OF \0% COMBUSTIBLE
MATTER WAS ADDED WHEN AN
AUTHOR INDICATED HIS VALUES
REPRESENTED ONLY ASH
EMISSION.
«• VALUES CHOSEN





















112
112
112
12


112
112
112
112
112
112
60
112
112

112
112
112
112
12
112
112
95


1



ME
112
112
1C
62









112
112
[95
66
56
112
58
116
61
62



56
58
117
61


NUMBERS IN BLOCKS ARE
REFERENCES CITED





i

5FJ| (il2] fr \\C>4 ,

               0


                 TOTAL PARTICIPATES AS  PERCENT OF ASH IN COAL BURNED


               Figure 7-I7.   Particulate emissions from  cyclone  units.
 20'
 15-
  5-
                  I	1
                              A VALUE OF 50% COMBUSTIBLE MATTER WAS

                              ADDED WHEN AN AUTHOR  INDICATED HIS VALUES

                              REPRESENTED ONLY ASH  EMISSION.
                                  VALUE FOR UNIT WITHOUT REINJECT10N



                              r—\


                              L.j VALUE FOR UNIT WITH  REINJECTION
                              NUMBERS IN BLOCKS ARE


                              REFERENCES CITED
                               VALUE CHOSEN


                               WITHOUT ASH REINJECTION
                              58
                                                RVALUE CHOSEN

fnsfee]
118|l 19J71
58
23
58
80
71 !


MOI^Tl
58 !
23
._Si33
58 !
TO 261
                                          99
   20
         30
40    50   60    70    80    90   100   110    120   130

    TOTAL PARTI CULATES  AS  PERCENT ASH IN COAL
                                                                      HO
      Figure 7-18.  Participate emissions  from spreader-stoker-fired  units.
Particulate Emissions
                                                                71

-------
 Scattering of these data probably results from varying firing
 rates.   A value of 25 percent was chosen to represent any type
 of stoker other than spreader  stokers.
       A summary of the particulate emission factors,  expressed
 in terms of the ash content of  coal,  is shown in Table 7-8.
5-

im

67
81
96

67
66
47
95
58
80
•»
67
120
47
47
66
67
120
120
1 2O
47
tw
67
120
120
95
81
62
58
kLUE CHOSEN
A VALUE OF 40% COMBUSTIBLE MATTER WAS
ADDED WHEN AN AUTHOR INDICATED HIS VALUES
REPRESENTED ONLY ASH EMISSION.
120
63
64 I2o|67
"80 I67I I67I
23 1 |67|67l
o
o
                 30
         Figure 7-19.
                      40   50   60   70   80   90  100  110  120

                      TOTAL PARTICULATES AS PERCENT OF ASH
                                                             130  140  150
Particulate emissions from stoker-fired units
       (except spreader stokers).
   Table 7-8.  PARTICULATE EMISSION FACTORS FOR COAL
        COMBUSTION WITHOUT CONTROL EQUIPMENT
Type of unit
Pulverized
General
Dry bottom
Wet bottom without
fly-ash reinjection
Wet bottom with
fly-ash reinjection
Cyclone
Spreader stoker
without fly-ash reinjection
with fly-ash reinjectionb
All other stokers
Pounds of particulate
per ton of coal burned3
(Values represent emissions
before control equipment)
16A
17A
13A

24A
2A
13A
20A
5A
Percent of ash in
coal as particulate
emission
80
85
65

120
10
65
100
25
  ttThe letter A to be used for all units other than hand-fired equipment,  indicates
   that the percent ash in the coal should be multiplied by the .value given.  Example:
   If the factor is 17 and the ash content is 10 percent, the particulate emission
   before the control equipment would be 10 times 17, or 170 Ib participate/ton
   of coal.

  bValues should not be used as emission factors. Values represent the  loading
   reaching the control equipment always used on this type of furnace.
 72
                            EMISSIONS FROM COAL COMBUSTION

-------
Effect of Firing Rates on Emissions

      Emissions from stokers are greatly dependent on the
firing rate, as  shown in Figures 7-20 and 7-21.  Figure 7-20
            • FROM  REFERENCE NO. 67

            D FROM  REFERENCE NO. 8!
           0.1    0.2  0.3   0.4  0.5   0.6  0.7   0.8  0.9   1.0


                        GRATE LOADING, ,I06 Btu/ft2 - hr


  Figure 7-20.  Effect of firing rate on parti cul ate emissions from large
                     underfeed-stoker-fi red  units.


Particulate Emissions
1.1
73

-------
shows the total particulate emission, expressed as a percentage
of the ash in the coal, as a function of the grate heat release.
The data were taken from two references, both representing
large underfeed stokers.  Many authors have reported stack
concentrations as a function of the  grate loading, but these data,
as explained earlier, were too diverse to permit definite con-
clusions and did not include information on ash in the coal fired.
Figure 7-21  shows trends in emission rates for different types
of stokers.   This  figure might be used  to indicate the relative
discharge as burning rates increase, although it is not based
on fuel-ash content.
              I- o
              z o
                   3. 5
                   3.0
                   2. 5
                   2. 0
              O
              O CO
              £ ^  1.5

              1=3
              O LL.  1.0
              a: —
              
-------
   80

VS.
 ^ 60
_J
•a.
o
o
>- 40
a:
o
z
_ 20
                •SLAGGED  IN FURNACE
                                              EMI TIED
                                             AS FLY  ASH
                              EMITTED  DURING SOOT BLOWING
               25
                        50        75       100
                           PERCENT LOAD
                                                   1 25
               Figure 7-22.  Participate emission
               versus load for a slaq-tap furnace. *
                25
                         50
                                    75
                                            -100
                                                      125
                              PERCENT LOAD
               Figure 7-23.  Particulate concentration
               in stack gas versus load for a slaq-tap
               furnace96 (at stack C02 concentrations).
                                        i
      Although the number of hand-fired units in urban areas
is rapidly diminishing and this  mode of combustion is usually a
minor contributor, data to determine a representative emission
factor are given in Table 7-9 so that the presentation of emis-
sion factors is complete.

      From these data,  it is estimated that approximately 1  per-
cent of the coal is emitted as particulate  matter from hand-fired
furnaces  and stoves.   This estimate is equal to about 0. 8 pound
per 10^ Btu, or  20 pounds per ton of coal burned.
Particulate Emissions
                                                       75

-------
  Table 7-9.  PARTICULATE EMISSIONS FROM HAND-FIR ED

                 COAL-BURNING EQUIPMENT
Reference
64
122
138
136
137
Particulate emission
As percent
of coal
1.85
0.7-1.7
0.8-2.5
1 -2
3
0.3
0.5
1.3
0. 1
As percent
of ash
69


17
22
3
Percent
combustible
in particulate
46

90
0
60
45
20
Remarks

Lighting fire
Refueling
Usual range
Burning
bituminous
Burning
s emibituminous
or anthracite
Burning
anthracite
Burning coke
Burning
subbituminous
CONTROL OF PARTICULATE EMISSIONS

      The influence of control equipment is often neglected by
persons making emission inventories.  The general level of
control of any community is determined by the quality of air
pollution control programs, the length of time they have  been
in existence,  the attitude of the citizeny toward the programs,
the prevailing methods of coal utilization,  and the  characteristics
of the coal used throughout the area.  All of these  factors,  applied
with judgment and skill as the emission inventory is developed,
will enhance the accuracy of a survey.

      The efficiency of particulate control  equipment for the  area
as a whole can be judged by looking at a number of typical units,
applying the factors for emission without control,  "plugging in1'
the regulatory limit of emission and the ash content of the coal
(see Table 3-6, chapter III), and calculating the efficiency  of
flue-gas-cleaning equipment to meet the air pollution regulations.
76
EMISSIONS FROM COAL COMBUSTION

-------
      Example:  The local ordinance in effect at the time the
 plant was built placed the emission limit for particulates at
 1 pound per million Btu input.  The  plant under consideration is
 a spreader stoker with fly-ash reinjection, burning Illinois coal
 with  a  heat content of 13, 000 Btu per pound (dry basis).  From
 Table 3-6,  chapter III,  select 10 percent (dry basis) as the ash
 content.  According to Table 7-8, the emissions would be equal
 to 100 percent of the ash in the coal.  Since both heating content
 and ash content are on the same basis, the moisture content
 would affect both to the same degree and,  therefore, it can be
 considered as if it were an as-fired basis. The emission  from
 this unit without any control equipment would be
  1. 00 (ash out)(0. 10 Ib ash/lb coal)(lQ6 Btu)        _    .   6
 	7	  or 7.7 lb/10  Btu
          (13,000 Btu/lb coal)( 10  Btu)
The collection efficiency of (1   1/7.7)  x. 100 or,  87 percent,
would be necessary to comply with the ordinance.

      Most coal-burning plants have some type of control equip-
ment,  ranging from the settling-chamber effect of large breeches
and chimney bases to a combination  mechanical-electrical pre-
cipitator for large central stations.  The efficiency of each type
of collector depends  primarily upon  the size, specific gravity,
and resistivity of the particles acted upon.  In general, the
smaller the unit is, the less the total emission and the larger
the particle size.   As unit size increases, the total quantity of
particulate carried to the collector increases and particle size
decreases; therefore, the need for more efficient gas-cleaning
equipment is compounded.  Table  7-10 delineates operating
conditions and use limitations for  major categories of particulate
collectors. Efficiency ranges generally achieved by commonly
used collectors on various units are  given in Table 7-11.

      No generalization can be made for collection efficiency
values to be expected for any specific unit.  In making an emis-
sion inventory,  one looks at local  codes and ordinances to estab-
lish maximum allowable emissions for that community.  Then,
using emission factors for uncontrolled equipment established
in this report, the emissions from each type of unit are calculated.
If the calculated values are greater than the prevailing codes, it
can be assumed that control equipment is being used.  It can
usually be assumed that the emissions are equal to or less than
the prevailing codes, and in some  specific cases, much less.

Particulate Emissions                                      77

-------
~J
CO
              Table 7-10.  DUST COLLECTORS FOR COAL-FIRED HEATING AND POWER PLANTS32
H



to

S

to





g

O
O

i
tu
cj
to
H
i—i

§
Collector
Type
Cinder trap
Medium draft
loss
Single cyclone
(large diameter)
Multicyclone
(small diameter
tubes)
Wet scrubber
Electrostatic
precipitator
Siliconized glass
filter
Collecting
action
Gravity
Inertia
Centrifugal force
and inertia
Centrifugal force
and inertia
Gravity
Electrical
attraction
Filtering
Recommended
application
Smaller plants with under-
feed, vibrating, chain, and
traveling-grate stokers
Smaller plants with very
critical on-grate firing
On-grate firing at high
rates and some spreader
stokers
Spreader stoker
Spreader stoker and pul-
verized-coal-firing units
Pulverized-coal-firing unit
Pulverized-coal-firing
units
Efficiency relative
to particle size
30 to 40% for 45 \j.
and smaller; 75%
or more for
particles over >
45 PL
Overall - to 65%,
100% over 2 5 -pi
size
50 to 90% for
particles over
ZO (i
75 to 90% for
particles over
10 pL
70 to 90%, depend-
ing on particle
size; 75% over
2n
85 to 99% - < 1
to 10 IL (high effi-
ciencies call for
series installation
with multicyclone
collector)
98 to 99% for < 1
to 44 (i
Draft loss,
inches of water
0. 1 to 0. 5
(natural draft
usually
sufficient)
0. 4 to 1.5
0. 5 to Z. 0
2. 0 to 6. 0
13 to 20
0. 1 to 0. 5
1 to 6
Other considerations
Used mainly to elimi-
nate cinder nuisance
in immediate plant
area.
Abrasion may occur:
made in variety of
designs to fit job.
Made in variety of
designs. Care re-
quired to fit design
to job.
Abrasion may be a
problem.
Caking and corrosion
may be a problem,
also water recovery.
Continuous cleaning
necessary.
Exit temperature
limited to 600° F

-------
   Table 7-11.  USUAL EXPECTED EFFICIENCY RANGES FOR
       COMMONLY USED CONTROL EQUIPMENT (percent)
Type of firing
or furnace
Cyclone
Pulverized
Spreader stoker
Other stokers
Type of control equipment
Electrostatic
precipitator
65-99a
80-99. 9*


High-
efficiency
cyclone
30-40
65-75
85-90
90-95
Low-
resistance
cyclone
20-30
40-60
70-80
75-85
Settling chamber,
expanded
chimney bases


20-30
25-50
     The higher efficiencies can only be attained with high-efficiency cyclones in
     series with electrostatic precipitatoi's.
      For those areas where specific emission limitations are not
known or cannot be determined, average control practice  based
upon the present American Society of Mechanical Engineers Example
Ordinance, ^^ i. e. ,  0. 85 pound of particulates per 1, 000 pounds of
flue gases at 50 percent excess air,  can be assumed to be applicable.
For areas of better-than-average  control practice, consideration
might be given to applying one of the emission limitations considered
by the Subcommittee of the American Society of Mechanical Engineers
Committee on Air Pollution Control.  Figure 7-24 contains one of
                  1 ^ c
those considered. 1^-J

VARIABLES AFFECTING EFFICIENCY OF CONTROL
EQUIPMENT
      Many variables other than particle  size and density affect
the collection efficiencies.  For centrifugal collectors,  the
efficiency of collection increases as load increases (Figure 7-25),
whereas the reverse is true for electrostatic precipitators.
Thus, the centrifugal collector tends to improve its efficiency
with increasing exit gas loadings,  which are associated with
increased boiler load, thereby tending to maintain a constant
emission concentration at the outlet of the collector.  Conversely,
as the load increases, the efficiency of an electrostatic precipitator
decreases,thus  total emissions are increased.  For example,
assume that the efficiency curves  in Figure 7-25 represent a unit
that generates  7 pounds of flue  dust per 10° Btu at 50 percent load
and 10 pounds of flue dust per 10°  Btu at 100 percent load at  the
collector inlet.  Emissions from the centrifugal collector will be
1.75 pounds per 10° Btu for either load, whereas the emissions
from the electrostatic precipitator will be 0. 21 pound per 10° Btu
for a 50 percent load and 0. 5 pound per 10° Btu for a 100  percent
load,  a 240 percent increase in particulate emission.
Particulate Emissions
79

-------
       i2.0
       o
       a.
      1-^
      ll.O
       = 0.8
      -H
      m 0.6
        0.2
                            PRESENT ASME MODEL
                                                             10'
      IO6        IO7        IO8        IO9       lo'°
                         INPUT, Btu/hr
Figure 7-24.  Proposed revision  to ASME model ordinance for
             permissable fly-ash emissions  '" (At the present
             time the ASME Air  Pollution  Standards Committee
             is considering proposals for the control  of  dust
             emission from combustion equipment that differ
             from those shown above.)
     100


      95
    s.

    \ 90
    U


    I**
    c
    3

    3 80
    j
    5
    i

      75
                  -CENTRIFUGAL, ELECTRICAL  SERIES UNIT
              _  ELECTRICAL PRECIPITATOR
                   CENTRIFUGAL COLLECTOR
                             j	I
                                           I
                                                  I
                50     60    70     80    90
                              PERCENT LOAD
                                           100    110
                Figure 7-25.  Typical  performance curves for
               fly-ash collectors serving large pulveri zed-
                         coal-fired furnace.''1*

       The carbon content in the  fly ash affects the collection
efficiency of both centrifugal and electrostatic precipitators.
An increase in carbon content is usually associated with an
80
                            EMISSIONS FROM COAL, COMBUSTION

-------
increase in size distribution and electrical resistivity, and a
decrease in specific gravity.  In general,  the centrifugal col-
lector becomes more efficient because of particle size increase
as the carbon content increases, and the electrostatic precipita-
tor becomes less efficient because of the increase in electrical
resistivity.    Electrostatic precipitators are not generally used
for high-carbon ash,  such as  that derived from stokers,  because
the particles lose their charge too rapidly.
Particulate Emissions                                        81

-------
                     CHAPTER  VIII.
                GASEOUS  EMISSIONS
            FROM  COAL  COMBUSTION
SULFUR OXIDES

Theoretical Considerations

      The sulfur content of coal ranges from less than 1 percent
to greater  than  10 percent (by weight).  During combustion, a
high percentage of the sulfur  in coal is oxidized to sulfur dioxide
(SO2) or sulfur trioxide (803).  Some  of the sulfur oxide (SOX)
complexes •with fly ash and ash residue or slag, but most is
emitted as a part of the stack gases.  If combustion is very
inefficient,  hydrogen sulfide (t^S) may be evolved.  The oxida-
tion of sulfur to the  sulfur oxides  is similar to  the oxidation of
carbon.  If large amounts  of carbon monoxide are detected, one
might suspect the presence of I^S. The majority of the sulfur
should, however, be oxidized to SC>2 in modern furnaces.

      The amount of sulfur emitted as SC>2 may be inferred from
a material balance.  The total sulfur effluent is emitted from the
chimney as  a gas or in the particulate matter,  or is removed
after combination with the slag or  ash residue. Data compiled
in reference 126 show that about 2 percent of the sulfur goes  to
the fly ash and soot  (Figures  8-1 and 8-2).   Figure 8-3 shows
that less than 1  percent of the sulfur usually goes into the slag
or residue, whereas data in Figure 8-4 indicate that 1 to 2 per-
cent of the sulfur usually goes to SOj.  Thus, if no appreciable
amount of I^S is formed, about 95 percent of the  sulfur is
emitted to the atmosphere as  SC^.

Emission Data

      Attempts were made to  separate the data for various
classes of equipment and to find other relationships that might
account for large differences  in the amount of sulfur going to
products other than SO2.  One author reports that stoker-fired
units emit from 65 to 75  percent of the sulfur as SO2, whereas
pulverized-fuel-fired units emit as much as 95  percent of the
sulfur. 13 Such values cannot be confirmed by other information

                              83

-------
20-
i f\m




1 Ctm



























D

















i i ^
•'•'•'•
! i i
***!















)
















/







m









ALL VALUES TAKEN FROM REFERENCE 126
EXCEPT WHERE INDICATED.
[§|] VALUES FROM LOCOMOTIVES126

| J OTHER SOURCES









;;S; p gs |:;j;SJ
H;: :;j;g m 83 |'2v| [127 12?
§11 Hll 3* 11 > HI • iii
6 8 10 12 14 16 33 40 42 4
               SULFUR  IN COAL FOUND IN  PARTI CULATE EMISSIONS,

           Figure 8-1.  Percentage of sulfur in coal  found in
                       parti cul ate emissions.
reported in the literature.  It is  of interest to note that Figures
8-1 through 8-3 show values in excess of 10 percent of the sulfur
in the fly ash and slag.  No reason for these high values could
be established except that data from  references 127 and 129 were
for the  combustion of coke in hand-fired stoves.   Many of the  high
values for sulfur in the slag were from coal combustion in loco-
motives,  and the low values for gaseous sulfur products were
also from locomotives (Figure 8-5).   This seems to indicate that
inefficient combustion might direct more  sulfur into the slag than
would efficient  combustion.

      All of the values found in the literature for the proportion
of the sulfur in the coal emitted as SC>2  are shown in Figure 8-5.
These data are for equipment ranging in size from domestic
stoves to large steam-electric power plants.  Only the values for
the locomotives were consistently lower than those previously
84
EMISSIONS FROM COAL, COMBUSTION

-------
  50-
  45- ,
   25.
   15.
S.
  10'
                    ALL VALUES  TAKEN FROM REFERENCE 126
                  6   8    10   12   14    16   18

                     S03 IN  PARTICIPATE EMISSIONS, %
                                                 20   22   24   26
        Figure 8-2.  803  content of the parti cul ate emissions.
determined by a material balance.  Previous experience with the
material balance for sulfur oxides emissions135 indicated that the
measurement of SOX by itself is not always a true representation
of the SOX emission.  The measurement of SOX must be accom-
panied by a complete material balance to confirm the measured
gaseous value.   For the above reasons,  a value of 95 percent of
the sulfur in the coal is chosen for the emission of SO2 from the
stack, and a value of 1 percent of the sulfur in the coal is selected
for the emission of SOj.

      One of the reaction products of sulfur,  hydrogen sulfide, has
been given little consideration in the study  of coal combustion.
One author  reported he found an average of 0. 4 percent of the
sulfur in the coal converted to H2S in a hand-fired stove,  whereas
only a trace of H2S was found from the burning of coke. 129
Gaseous Emissions
                                                              85

-------
          128
          128
          128
          128
                          j   | "T-inV VY RO •
                                            m
                                                           24    26   28    30   32
                             SULFUR  IN  COAL  FOUND  IN  SLAG,
           Figure 8-3.  Percentage of sulfur in coal  found in slaq.
                       10
NUMBERS -IN BLOCKS ARE
REFERENCES CITED
104
62
62
62
128
128
128
128
126
126
126
126
104
131
132
129
129
133
89
134
130
126

104
126
126
126
126
126
126
Il04
I04|126
13
i 69 I . i
                       " 0     2     4     6     8    10
                                 SULFUR  IN COAL
                               EMITTED AS  S03, %

                  Figure 8-4.  Percentage of sulfur in coal
                             emitted as SO^.
86
EMISSIONS FROM  COAL COMBUSTION

-------
Zb"
20-
co
LU
1^
— J

^0.4, and N2O5 but calculated as  NO2- During combustion,  oxygen
and nitrogen gas combine to form nitric oxide (NO) as follows:
Gaseous Emissions
S7

-------
                       0
                         2
            2 NO
(1)
If time permits , reaction (1) continues to equilibrium, butitdoesnot
go to completion as does the carbon to carbon dioxide reaction.  The
NO will, however, react with more oxygen and form nitrogen dioxide
(NO^) and other nitrogen oxides. The N£ to NO equilibrium may shift in
either direction, depending upon many variables. If the concentration
of one of the gases is increased,  the equilibrium shifts to the opposite
side. There is anabundance of nitrogen butvery little oxygenpresent
for this reaction. If the amount of oxygen (excess air) is increas ed with-
out reducing the flame temperature, the NO concentration will also in-
crease, and the reverse is true.  As the NO reacts with oxygen to produce
NO2, there is a reduction in the concentration of NO, which removes it
from the equilibrium in reaction (1) above. The NO is replaced by re-
action (1) returning to equilibrium.
      Other variables that affect  this equilibrium are the  different
temperature, pressure, and concentration zones through which
the gases pass.  Most of the NO is formed in the flame, where
very high temperatures  are  present.   The residence time of the
gases at this temperature, however,  is  relatively short,  and the
NO reaction  is prevented from  reaching equilibrium.  Figure 8-6
shows  the  theoretical concentration of NO, assuming typical fuel
analysis,  typical excess air, and a residence time of 0. 5 second
at various flame temperatures. 136
       1,000
         800
         600
         200
         2,800
3,000           3,200
  FLAME TEMPERATURE, °F
    3,400
       Figure 8-6.  Theoretical formation of nitric oxide versus flame
                          temperatu re. 136
88
EMISSIONS FROM COAL COMBUSTION

-------
      The main factors in NOX production are:  the flame and
furnace temperature,  the length of time that combustion gases
are maintained at this flame temperature,  the rate of cooling of
the gases,  and the amount of excess  air present in the flame. 104,
105,106, 135

Emission Data

      Very little  stack-sampling data on oxides of nitrogen in
coal burning plant emissions have been reported in the literature.
From the theoretical considerations, one might expect lower
flame temperature to be found in domestic  units and higher flame
temperature to be found in pulverized fuel  units.   Woolrich^^
proposed a method for estimating NOX emissions from coal com-
bustion based on  an empirical approach using data from  the  com-
bustion of oil and gas.  His resulting equation is:
                                            1 18
          T-,    j  -*T^  /T       Btu/hr input
          Pounds NO  /hr      	c—
                    x
                               3.8 x  10
                                        6
(2)
When NOX emission data for oil and gas 138 are plotted on six-
cycle log-log graph paper,  the data tend to follow a straight line,
as represented by equation (2), but with a different denominator.
If, however, these emission data were presented as pounds of
NOX per 10° Btu input (instead of pounds NOX per hour) versus
10° Btu per hour, the data  stay in a consistent order of magnitude
(approximately 0.1 to 1.0 pound NOX per 10° Btu),  but do not
follow any real relationship.  This lack of correlation results
from the many factors involved in the production and decomposi-
tion of the oxides of nitrogen.  Equation (2), however, does
permit the selection of an emission range.

      Three  articles report ranges of concentrations representa-
tive of large power plants,  100 to  1,400 ppm69' 132 and 650 to
1,460 ppm.   '  When these concentrations were standardized to
a stack gas containing 12 percent CO2 from a bituminous  coal,
they represented emission  ranges of 0. 17 to 2. 5 and  1. 1 to 2. 6
pounds per 10& Btu, respectively. Two authors, referring to
data similar to the above along with oil and gas data, derived
NCx emission factors of 0. 01 pound of NOX per pound of c
and 0. 004 ton NOX per ton of coal, 1^1 values that are equivalent
to about 0. 8  and  0. 3 pound  of NOX per 106 Btu, respectively.
There is an indication that  small  units (commercial and domestic)
may emit less NOX than large units (see  Tables 8-1 and 8-2).
One author confirmed the above supposition by measuring NOX
emissions  of from 0. 0014 to 0. 047 pound per 106 Btu from a.
                           i OQ
domestic stove in England.  l  '

Gaseous Emissions                                          89

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  Table 8-1.  EMISSION OF NITROGEN OXIDES FROM UNITS
                                               i
                 FIRING COAL IN SUSPENSION



Test



Full
loada





Partial
loadb



Burner configuration
or type
Vertical
Corner
Front wall
Spreader stoker
Cyclone
Horizontally opposed
Vertical
Corner
Front wall
Spreader stoker
Cyclone
Horizontally opposed
NO , lb/10 Btu
X
Before fly-ash
collector
0. 38
0.95
0. 68
0. 65
2.5
0. 65
0.28
0.73
0. 82
0.73
1.9
0.66
After fly-ash
collector
0. 55
0.71
0. 95
0.76
2.2
0. 59
0. 31
0. 57
0. 74
0. 68
1.8
0. 56
Average values for three or four tests at each unit.
Average values for two tests at each unit.
        Table 8-2.  EMISSIONS OF NITROGEN OXIDES

                   FROM SMALL UNITS47
              (3x10  Btu/hr input or smaller)
Type unit
Underfeed stoker
Underfeed stoker
Hand-fired stoker
NOX,
lb/106 Btu
0.30
0.36
0. 11
Size of unit,
106 Btu/hr
3
0.066
0. 115
      In view of the limited data available,  arriving at a suggested
emission factor for oxides of nitrogen is difficult; however, the
90
EMISSIONS FROM COAL COMBUSTION

                            GPO 825-629-7

-------
 following factors are suggested,  pending the development of a
 more reliable body of data:

      0. 8 pound NO  /10^ Btu for large units (10^ or more Btu
      per hour input)

      0. 2 pound NO  /106 Ecu for small units (less than 106 Btu
      per hour input)
OTHER GASEOUS EMISSIONS

      Some work has been reported for gaseous emissions other
than SOX and NOX.   These values are shown in Tables 8-3 and
8-4.  Data used to determine a heat balance can also be found in
the literature.  These data are old and/or refer to hand-fired
units (see references 49, 50, 67,' 129,  142, 143).   The values
given by these data are not thought to be representative of those
found today.  If values for carbon monoxide (CO),  hydrocarbons,
or formaldehyde are needed, one can judge from the above data
       Table 8-3.   COMBUSTIBLE GASEOUS EMISSIONS
             FROM SUSPENSION-FIRED UNITS1  4
Type of boiler firing
Vertical

Corner

Front-wall

Spreader -stoker

Cyclone
Horizontally opposed
Emissions, lb/10 Btu
CO
0.017

0.011

0.005

0.029

-
0.044
Hydrocarbons
0.010

0.004

0.010

0.009

-
0.001
Formaldehyde
2.5 x 10"4
_4
1.7 x 10
_4
1. 4 x 10
.4
0.6 x 10
_4
1.7 x 10
1.0 x 10"4
 Gaseous organic gases at room temperature expressed as a
 single carbon atom hydrocarbon, measured using infrared
 and flame ionization techniques.
Gaseous Emissions
91

-------
 what might be expected.  Formaldehyde seems to be consistently
 about 0. 0002 pound per  106 Btu, whereas  both CO and hydro-
 carbons vary 3 to 4 orders of magnitude.  Suggested estimating
 factors are shown in Table 8-5.
    Table 8-4.  COMBUSTIBLE GASEOUS EMISSIONS FROM
                    GRATE-FIR ED UNITS47
Type unit
Chain grate
Spreader stoker
Underfeed stoker
Underfeed stoker
Underfeed stoker
Hand-fired stoker
Size (infant),
106 Btu/hr
147
59.2
4.4
3.0
0.066
0. 115
Emissions, lb/106 Btu
CO
0.51
<0. 1
0. 16
0. 14
1. 1
3.5
CH4
0.005
0.006
0. 116
0.036
0. 12
0.73
Formaldehyde
1.4 x 10-*
2.Z x lO-4
2. 1 x lO-4
3.8 x lO-4
-

           Table 8-5.  SUMMARY OF COMBUSTIBLE
                GASEOUS EMISSION FACTORS
Source
Power plants
Industrial stokers
Domestic units
Emissions, lb/10 Btu
CO
0.02
0. 1
2
Hydrocarbons
0. 007
0.05
0.5
Formaldehyde
2 x 10"4
2 x 10"4
2 x 10"4
      Another pollutant of possible importance is hydrogen
chloride (HC1).  As shown in chapter III,  chlorine occurs in coal
in concentrations of about 0. 1 percent.  Calcium chloride may
also be added in concentrations of 0. 1 to  0. 5 percent as an anti-
freeze or dust-proofing agent. ** If all of this were emitted as
HC1,  then from 0. 08 to 0. 3 pound of HC1  per  106 Btu might be
emitted.  One author  recorded a concentration of 49 ppm HC1 at
stack conditions when burning a coal containing 0. 066 percent
chlorine.      This value  corresponds  to about 60 percent of the
chlorine being emitted as HC1.
                       EMISSIONS FROM COAL COMBUSTION

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                       CHAPTER  IX.

FUTURE NEEDS FOR DATA  AND RESEARCH


 EMISSION DATA NEEDS

       This report presents emission factors based on existing
 data, which are, in many instances, meager.  Much of the data
 in the literature could not be used because the  information neces-
 sary to calculate a useful emission factor was  not reported.  Re-
 finement of the emission factors presented in this report could
 be expedited if future reported stack sampling  is accompanied by
 a complete material balance and a good description of both the
 sampling equipment used and plant operating conditions that
 existed at the time of sampling.   If sampling data were presented
 in this manner, the following needs for more emission data could
 be satisfied:

       1. The establishment, by types of equipment, of emission
          values for nitrogen oxides, carbon monoxide, hydro-
          carbons, and soiling potential.

       2. The effect of design variables on emissions of nitrogen
          and sulfur oxides, particulates, hydrocarbons,  and
          soiling potential.

       3. The effect of various types of control  equipment on emis-
          sion of particulates, sulfur oxides,  nitrogen oxides,  and
          hydrocarbons.

       4. The actual operating characteristics of emission control
          equipment compared to its design criteria.


 RESEARCH NEEDS

       During the past several decades, coal-burning equipment
 has been markedly improved,  and many substandard plants have
 been replaced  by plants fired with other fuels.  A coal-fired
 plant with maximum controls can compete favorably in many
 respects with one fired with fuel oil, but it cannot match the
 performance of a gas-fired plant as judged by the air pollution
 potential of the combustion products.
                              93

-------
      Intensive research effort is needed to create the technical
capability of matching the air pollution potential of coal combus-
tion to that of any fuel.  It can be done; and unless it is done,
there will always be the temptation to require by ordinance
(directly or indirectly) the least offensive fuel in the interest of
community welfare.

      In the immediate future, the areas in which the overall
emission potential of coal could be reduced include:

      1. Improvement of coal quality by lowering the ash and
        sulfur content; producing sizes more acceptable to the
        firing equipment; and expanding the availability of low-ash,
        low-sulfur coals at attractive prices (see reference  144).
      2.  Improvement of fuel-burning equipment as follows:

         a.  Over-fire air systems should be made more effective,
            should have better controls, and should provide for
            better combustion at low loads.

         b.  Equipment should be improved to reduce  or prevent
            formation of nitrogen oxides.

         c.  Boilers  should be so designed so that soot blowing is
            either not necessary or may be accomplished without
            overloading particulate collectors, and overall effi-
            ciency should be improved to reduce fuel requirements.
      3.  Development of better air cleaning equipment.  Reliabil-
         ity and efficiency of existing particulate removal equip-
         ment should be improved.  Uses and markets for con-
         taminants collected should be developed to ease the
         economic burden of collection.  New, more practical
         systems  for reducing sulfur- and nitrogen-oxide emis-
         sions, or methods for preventing their formation during
         the combustion process should be devised.


      The development of a long-range effort should include
consideration of new concepts of burning coal, such as gasifica-
tion or liquifaction.  In another direction,  continued improve-
ment in the heat rate of central steam-electric generation and
reduction of electricity transmission costs could result in re-
                                                /    '
placement of thousands of small,  poorly controlled sources with
a single  coal-burning plant with highly efficient emission control.

94                     EMISSIONS FROM COAL COMBUSTION

-------
SUGGESTED RESEARCH DIRECTIONS

      The literature reviewed in preparing this report gave
some insight into the direction future research might proceed.
Much of the current research on control of sulfur oxides is
directed toward either collecting sulfur oxides in the stack gases
or removing sulfur from the coal.   Some of the reports studied
indicate a possibility of tying up the sulfur in the slag.  This
might be done by a two-stage combustion operation in which the
first stage maintains a highly reducing atmosphere and the
second  stage completes  combustion.  Examples of similar oper-
ations are  the blast furnace and the kraft paper mill recovery
furnace.

      Oxygen could replace combustion air and be used in  con-
junction with the above method or be used only as a means of
reducing the volume of stack'gases to make treatment of such
gases more economical.

      The nitrogen oxides data indicate that emissions could
possibly be reduced by changing burner positions.  Staged com-
bustion and very low excess air might yield better results  than
those from changing burner configuration.   The replacement of
combustion air by pure oxygen would, of course, essentially
eliminate emissions of nitrogen oxides.

      More effective particulate control might be accomplished
by a change in furnace or burner design.  Data examined in pre-
paring this report indicate that actual operating efficiencies of
control equipment are not close enough to design efficiencies.
With expectations of more stringent air pollution ordinances,
application of fabric filtration to particulate emission control
may become desirable.  Such possible use should be studied.

      Since the day coal was first fired,  it has created significant
air pollution.  Although much progress has been  made toward
control, it is unlikely that tomorrow's cities will tolerate emis-
sions experienced today from coal combustion.
Future Needs for Data and Research                         95

-------
                      REFERENCES
 1.   Bituminous coal facts.   National Coal Association.
     Washington,  B.C.  1964.

 2.   Hubbert, M. K.  Energy resources.   A report to the Com-
     mittee on Natural Resources of the National Academy of
     Sciences.  Washington,  D.C.  1962.

 3.   Keystone coal buyers manual.   McGraw-Hill, Inc. New York.
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 4.   Bituminous coal and lignite changing patterns in distribution
     and markets , 1960-1962.  Mineral Industry Surveys .  U.S.
     Department of the Interior, Bureau of Mines. Washington, D.C.
     May 1963.

 5.   Keystone coal buyers manual.   The American Retail Coal
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 6.   Steam-electric plant factors 1961.  National Coal Association.
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 7.   Aresco,  S. J. ,  J. B.  Janus, and F.  E. Walker.  Analyses
     of tipple and delivered samples of coal collected during
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 8.   Aresco,  S. J. ,  C.  P.  Haller,  and R. F. Abernethy.  Analy-
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     Department of the Interior, Bureau of Mines. 1959.

 9.   Aresco,  S. J. ,  C.  P.  Haller,  and R. F. Abernethy.  Analy-
     ses of tipple and delivered samples  of coal collected during
     fiscal year 1961.  Report of Investigations  6086.  U.S.
     Department of the Interior, Bureau of Mines. 1962.

10.   Fieldner,  A. C. ,  W. E.  Rice,  and H.  E. Moran.  Typical
     Analyses of Coals of the United States.  Bulletin 446.
     U.S. Department of the Interior,  Bureau of Mines.   1942.
                               97

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11.   Johnson, A. J., andG. H. Auth. Fuels andcombustionhandbook.
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12.   Perry, J.  H.  Chemical engineers' handbook.  4th ed.
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13.   Gould,  G.  Solving your air pollution problem.  Power.
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14.   Gunn, D. C. , and P.  G. W. Hawksley. Means for prevent-
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15.   Rohrman,  F. A. , and J. H. Ludwig.   Sources of sulfur
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17.  Orning,  A. A.  Industrial sources of air pollution (3) - Elec-
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18.  Glenn, R.  A. , and R. D. Harris.  Liberation of pyrite from
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20.  Fieldner, A.  C. ,  and W. A.  Selvig.  Fusibility of ash from
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21.  Marks,L. S. Mechanical engineers ' handbook.  5th ed. McGraw-
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22.  Nicholls, P., S.  B.  Flagg,  and C.  E. Augustine. Five hun-
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98                       EMISSIONS FROM COAL COMBUSTION

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23.  Rowley, L. N. ,  and J. C.  McCa.be.   Clean air - The engi-
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24.  de Lorenzi, O.   Combustion engineering.  1st ed.  Com-
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25.  North American combustion handbook.  1st ed.  North
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26.  Coal utilization manual.  American Coal Sales Association.
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27.  Faith, W. L.   Air pollution control.  John Wiley and Sons.
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28.  Magill, P.  L. ,  F. R. Holden,  and C. Ackley. Air pollution
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29.  Benton,  E.  D.  Application of over-fire air and its relation
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30.  Berl, E.  Smoke seen thru the eyes of a chemist.  Proc.
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34.  Katz, M.  Some aspects  of the physical and chemical nature
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35..  Engdahl,  R. B.  Combustion in furnaces and incinerators.
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References                                                  99

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37.   Kreisinger, H. ,  C. E. Augustine, and K. V.  Ovitz.  Com-
     bustion of coal and design of furnaces.  Bulletin 135.  U. S.
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38.   Kudlich, R.  Ringelmann smoke chart.  Information  circular
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40.   Hemeon, W.  Determination of smoke concentration by filter
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41.   Gruber, C.  W. ,  and E. L. Alpaugh.  The automatic  filter
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42.   Gruber, C.  W. ,  and C. E. Schumann.  Soiling potential - a
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43.   Recommended standard method for continuing air  monitoring
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44.   Proposed method of test for smoke density in the flue gases
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45.   Gruber, C.  W.   A smoke  abatement  survey of the City of
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46.   Cross,  R. C. , R.  A.  Sherman,  and H.  H. Ostborg.  Afield
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47.   Haugebrauck, R. P. ,  D. J. von Lehmden, and J.  E. Meeker.
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48.   Stoecker, W.  F.  Correlation of solids conte/nt in  gas with
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100                      EMISSIONS FROM COAL COMBUSTION

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49.  Smoke and its measurement; the correlation of optical density
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50.  Hurley, T.  F.  The composition of smoke.  Proc. National
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53.  Technical manual on single retort underfeed stokers.  JAPCA.
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54.  Application of over-fire air jets  to prevent smoke from sta-
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55.  Grimberg,  I.  Use nomograph to  find required. .. excess air
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56.  White,  H. J.  Effect of fly  ash characteristics on collector
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57.  Anonymous abstract.  Battle report on pollution control.
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59.  Gould,  G.  Dust collection methods for steam power plants.
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60.  Tigges, A.  J. ,  and H. Karlsson.  Lower flue-gas exit  tem-
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61.  White,  H. J.  Effect of fly ash characteristics on collector
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References                                                 101

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62.  Private communication with various companies listed in
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66.  Swengel,  F. M.   Correlation of data concerning spreader
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67.  Hardie,  P. H. , and W. S.  Cooper.  The  test performance of
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68.  Klemperer, H. ,  and J. E. Sayers.  Design aspects of an
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69.  Sensenbaugh, J.  D.  Air pollution problems  of public utili-
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70.  Flodin, C.  R. , and H. H. Haaland.  Some factors affecting
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102                      EMISSIONS FROM COAL COMBUSTION

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74.  Marks, C. H. ,  and E. R. Kaiser.  Reducing flue-dust emis -
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 104                    EMISSIONS FROM COAL COMBUSTION

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References                                                  105

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109.   Grunert,  A.  E.  What can power plants do about smoke
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112.   Collins,  W.  I.  Small and medium-size cyclone-furnace
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 106                      EMISSIONS FROM COAL COMBUSTION

                                                        GPO 825—629—3

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121.  Blackie, A.  Atmospheric pollution from domestic appli-
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References                                                  107

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 108                      EMISSIONS FROM COAL COMBUSTION

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144.   Bull,  W. C.  The Spencer de-ashed coal process. Presented
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 References
                                                            109

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                  ACKNOWLEDGMENT
      Grateful acknowledgment is extended to William Bye, who
started the work on this report, and to Richard Wromble, who
helped in its early phases.  Thanks are also extended to
Donald  F. Walters of the Technical Assistance  Branch, Division
of Air Pollution, without whose guidance in the  preparation,
engineering review,  and editing of the final text this work would
not have been completed.

      Acknowledgment is also extended to Jean  J. Schueneman
and others of the Technical Assistance Branch for their efforts
in preparing this report.
      Some of the data used in this report were supplied by a
number of contributors.  The assistance of the following  organ-
izations is gratefully acknowledged:

Department of Safety, Bureau of Air Pollution Control and Heat-
   ing Inspection, Cincinnati,  Ohio

Department of Buildings and Safety Engineering, Bureau  of Air
   Pollution Control,  Detroit, Michigan

Department of Public  Safety, Division of Air Pollution Control,
   St.  Louis,  Missouri

Department of Service and  Buildings, Division of Building Inspec-
   tion, Bureau of Combustion Control, Dayton, Ohio

Bureau of Air Pollution Control, Indianapolis, Indiana

Tennessee Valley Authority, Knoxville, Tenn.

Bureau of Mines,  U. S.  Department  of the Interior, Washington,
   D. C.

The Air Pollution Control Association, Pittsburgh, Pa.

Pennsylvania Electric Co. ,  Johnstown, Pa.

Public Service Electric and Gas  Company, Maplewood, N. J.
                              Ill

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 Consolidated Edison Co. of New York,  N. Y. , N. Y.





 Baltimore Gas and Electric Co. , Baltimore,  Md.




 Combustion Engineering,  Co. ,  N. Y. ,  N. Y.





 The Babcock and Wilcox Co. , N. Y. , N. Y.




 Koppers Co. , Inc. ,  Baltimore, Md.




 Western Precipitation Div. ,  Joy Mfg.  Co. , Los Angeles,  Calif.





 Research-Cottrell,  Inc.,  Bound Brook,  N.J.





 APRA Precipitator  Corp. , N. Y. ,  Y. Y.




 American Air Filter Co. , Inc.  , Louisville, Ky.





 Aerotec Corp. , Greenwich, Conn.
112                     EMISSIONS FROM COAL COMBUSTION
                                                    GPO 825-629-9

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BIBLIOGRAPHIC:  Smith, W. S. ,  and C. W.  Gruber.
    Atmospheric emissions from coal combustion -
    an inventory guide.   PHS PUBL.  No.  999-AP-24.
    1966.  112pp.

ABSTRACT: Information concerning atmospheric
    emissions arising from the combustion of coal
    was collected from the published literature and
    other sources.  The  data were abstracted, as-
    sembled, and converted to common units of ex-
    pression to facilitate comparison and understand-
    ing.  From these data, emission factors were
    established that can be applied to coal combustion
    processes to determine the magnitude of air  pol-
    lutant emissions. Also discussed are the com-
    position of coal,  theory of coal combustion, emis-
    sion rates, gaps in emission data, and future
    research needs.
ACCESSION NO.

KEY WORDS:

   Coal

   Burning

   Emission

   Particles

   Gases

   Smoke

   Air pollution

   Combustion

   Devices

   Research
BIBLIOGRAPHIC:  Smith,  W. S. ,  and C. W. Gruber.
    Atmospheric emissions from coal combustion -
    an inventory guide.  PHS PUBL.  No.  999-AP-24.
    1966.  112 pp.

ABSTRACT: Information concerning atmospheric
    emissions arising from the combustion of coal
    was collected from the published literature and
    other sources.  The data were abstracted, as-
    sembled, and converted to common units of ex-
    pression to facilitate comparison and understand-
    ing.  From these data, emission factors were
    established that can be applied to coal combustion
    processes to determine the magnitude of air pol-
    lutant emissions. Also discussed are the com-
    position of coal,  theory of coal combustion, emis-
    sion rates, gaps in emission data, and future
    research needs.
ACCESSION NO.

KEY WORDS:

   Coal

   Burning

   Emission

   Particles

   Gases
   Smoke
   Air pollution

   Combustion
   Devices
   Research
BIBLIOGRAPHIC:  Smith,  W. S., and C. W. Gruber.
    Atmospheric emissions from coal combustion
    an inventory guide.  PHS PUBL. No.  999-AP-24.
    1966.  112 pp.

ABSTRACT:  Information concerning atmospheric
    emissions arising from the combustion of coal
    was collected from the published literature and
    other sources.  The data were abstracted, as-
    sembled, and converted to common units of ex
    pression to facilitate comparison and understand-
    ing.  From these data, emission factors  were
    established that can be applied to coal combustion
    processes to determine the magnitude of air pol-
    lutant emissions.  Also discussed are the com-
    position  of coal, theory of coal combustion, emis-
    sion rates, gaps in emission data,  and future
    research needs.
ACCESSION NO.

KEY WORDS:

   Coal

   Burning
   Emission

   Particles
   Gases

   Smoke

   Air pollution
   Combustion

   Devices

   Research

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