r/EPA
united states
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park NC 27711
EMB Report 80-BYC-9
August 1981
Air
Benzene Fugitive Leaks
Coke Oven By-Product Plants
Emission Test Report
Bethlehem Steel Corporation
Bethlehem, Pennsylvania
-------
DCN 81-222-018-01-17 EMB Report No. 80-BYC-9
EMISSIONS TEST REPORT
FUGITIVE EMISSIONS TESTING
AT THE
BETHLEHEM STEEL
BETHLEHEM PLANT
Prepared by:
D.P. Wiesenborn, J.I. Steinmetz, and G.E. Harris
RADIAN CORPORATION
8501 Mo-Pac Boulevard
Austin, Texas 78759
Prepared for:
U.S. Environmental Protection Agency
ESED/EMB (MD-13)
Research Triangle Park, North Carolina 27711
EPA Contract No. 68-02-3542
Work Assignment No. 1
ESED No. 74/4j
4 September 1981
-------
CONTENTS
Section page
1 Introduction 1
2 Summary of Results 2
3 Process Description 6
4 Methodology 10
4.1 Screening Procedures 10
4.2 Sampling Procedures 11
4.3 Analytical Techniques 14
5 Quality Control/Quality Assurance 15
5.1 Quality Control for Screening Procedures 15
5.1.1 Calibration Checks 15
5.1.2 Repeated Screenings 16
5.2 Quality Control for Analytical and Sampling Procedures ... 16
5.2.1 Blind Standards 21
5.2.2 Accuracy Checks 21
Appendix A 30
Appendix B 44
-------
FIGURES
Number Page
3-1 Wash oil scrubber configuration at Bethlehem Steel,
Bethlehem, Pennsylvania 7
3-2 Light oil recovery unit at Bethlehem Steel, Bethlehem
Pennsylvania 8
4-1 Sampling train for baggable source of hydrocarbon emissions .. 12
5-1 Repeated screenings at Bethlehem Plant for pump seal ID #98 .. 18
5-2 Repeated screenings at Bethlehem Plant for valve ID #114 19
5-3 Repeated screenings at Bethlehem Plant for valve ID #116 20
5-4 Mass spectrum of pure benzene on SP-2100/bentone column 22
5-5 Mass spectrum of liquid leak from PU-68 on SP-2100/bentone ... 23
5-6 Mass spectrum of liquid leak from PU-68 on TCEP 24
5-7 GC of liquid leak from PU-334 on TCEP 25
5-8 Mass spectrum of liquid leak from PU-334 on TCEP 26
5-9 Mass spectrum of liquid leak from PU-334 on TCEP 27
5-10 Mass spectrum of liquid leak from PU-334 on SP-2100/bentone .. 28
ii
-------
TABLES
Number Page
2-1 OVA screening value distribution: Bethlehem Steel,
Bethlehem, PA 3
2-2 Summary of benzene and nonmethane hydrocarbon leak rates
(Ibs/hr) from sampled sources: Bethlehem Steel,
Bethlehem, Pennsylvania 4
2-3 Comparison of benzene content in emissions and in liquid
lines: Bethlehem Steel, Bethlehem, Pennsylvania 5
5-1 Calibration checking of OVA and TLV 17
5-2 Liquid blind standard analysis results 21
5-3 Accuracy checks data listing 29
iii
-------
SECTION 1
INTRODUCTION
This report presents the results of testing for fugitive VOC (Volatile
Organic Compounds) and benzene emissions at the Bethlehem Steel plant in
Bethlehem, Pennsylvania. The testing was performed by Radian Corporation on
January 20 through January 28, 1981 .
This work was funded and administered by the Emission Measurement Branch
of the U.S. Environmental Protection Agency under Contract No. 68-02-3542. The
results of this testing may be used in support of a National Emissions Standard
for Hazardous Air Pollutants for benzene from coke oven by-products recovery
units in steel mills.
Potential sources of fugitive benzene emissions in the by-product unit
were screened with a portable hydrocarbon detector to estimate the frequency
of leak occurrence. The liquid and vapor benzene emission rates were quantified
by collecting and analyzing samples from leaking fittings. Also, liquid
samples were obtained from process lines to provide data on the proportion of
benzene in process lines relative to the proportion of benzene in the vapor
emitted from fittings on those lines.
The following sections present a summary of results, a description of the
process configuration, the testing methodology, and QA/QC procedures. Example
calculations and a full listing of data and other supplemental information
are included in the appendices.
-------
SECTION 2
SUMMARY OF RESULTS
This section presents a summary of the fugitive emission data gathered at
the Bethlehem Steel plant in Bethlehem. All data are presented in the form of
original data sheets in Appendix B.
The plant screening results are presented in Table 2-1. This table
presents the distribution of OVA readings for each source type.
The results of the baggable sampling are presented in Table 2-2. The
mass emission rates are presented in pounds per day for each source in terms of
both benzene and nonmethane hydrocarbons. Mass emission rates are also pre-
sented in terms of vapor phase and liquid phase emission rate. Each source
was rescreened immediately before and after bagging. The average of these
two values is also presented in Table 2-2 for both the OVA and the TLV.
A comparison of the benzene concentration in vapor-phase and total
emissions with the benzene concentrations in the liquid lines is presented in
Table 2-3. The benzene concentration in the vapor-phase leak and the total
leak (vapor plus liquid) is expressed as a ratio of the benzene emission rate
to non-methane hydrocarbon emission rate, since bag samples are diluted with
air. The benzolized wash oil samples are reported as having no detectable
benzene (less than 1 weight percent). The detection limit for benzene in
liquid samples analyzed by gas chromatograph can potentially be at the parts
per million level. It was decided early in the study, however, that only
those streams containing 1 weight percent benzene, or more, were of interest,
so no attempt was made to exactly quantify benzene concentrations below that
level.
-------
TABLE 2-1. OVA SCREENING VALUE DISTRIBUTION: BETHLEHEM STEEL, BETHLEHEM, PA.
OVA
FLANGES
SCREENING
VALUE
0
200
>
Total
(ppmv)
to 199
to 9,999
10,000
Sources Screened
#a
151
0
0
151
%b
100.0
0.0
0.0
100.0
THREADED
FITTINGS
# I
0 —
0
0 —
0
VALVES
//
98
9
1
108
%
90.7
8.3
0.9
100.0
PUMPS
SEALS
#
24
3
1
28
%
85.7
10.7
3.6
100.0
EXHAUSTERS
#
19
2
3
24
%
79
8
12
100
.2
.3
.5
.0
u>
a) # - number of sources in each category
b) % - percent of total sources screened
-------
TABLE 2-2. SUMMARY OP BENZENE AND NONMETHANE HYDROCARBON LEAK RATES (LBS/HR) FROM
SAMPLED SOURCES: BETHLEHEM STEEL, BETHLEHEM, PENNSYLVANIA
Block Valves
Control Valves
Pumps
Exhausters
a) Average of
b) This symbol
Sampling
Date
01/22/81
01/23/81
01/26/81
01/27/81
01/23/81
01/22/81
01/23/81
01/27/81
01/28/81
01/21/81
01/27/81
before and
indicates
c) I denotes Inboard seal
Source
ID
108
120
114
116
124
84
87
91
103
104
129
139
141
40
115
121
109-1°
98-0
109-1^
98-0d
26-1
334-1
27-0
333-,0
66-1
68-1
20
18
19d
20d
23
Mean OVA Mean TLV
Rescreening Rescreenin
Value Value
130
24000
2150
240
123
75
320
700
250
48
205
95
25000
250
325
5200
11500
21500
14000
16000
78
50000
20
6600
30
15
42500
87501
100001
34000
9500
345
10001
850
175
89
60
1335
1500
550
110
110
58
8851
1000
300
2950
8700
10001
8450
8801
362
10001
30
10001
38
15
10001
10001
10001
7701
8901
after sampling screening values
that no
data was taken
and 0 denotes outboard
in that
seal of
ig Benzene Leak Rates
Vapor
0.000000
0.032253
0.001975
0.000000
0.000000
0.000000
0.000129
0.002389
0.000141
0.000290
0.000009
0.000055
0.021884
0.000000
0.000286
0.002774
0.079925
0.077834
0.072369
0.063723
0.002365
0.203298
0.000119
0.284684
0.000740
0.000152
0.173869
0.200168
0.154939
0.021283
0.000648
(given In
category.
Liquid Total
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
8
0
0
0
0
0
0
0
0
0
.000000 0.
.104944 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.845081 9.
.000000 0.
.405399 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
.000000 0.
000000
137197
001975
000000
000000
000000
000129
002389
000141
000290
000009
000055
021884
000000
000286
002774
079925
077834
072369
063723
002365
048379
000119
690083
000740
000152
173869
200168
154939
021283
000648
Nonraethane-HC Leak
Vapor
b
t
0.002419
0.000309
0.000000
0.000000
0.000397
0.003113
0.000262
0.000462
0.000046
0.000118
0.032042
0.000010
0.000656
0.003543
.
.
0.112669
0.094001
0.003256
0.171420
0.000259
0.291111
0.001016
0.000240
0.493436
0.379242
0.053182
0.002784
Liquid
0.000000
0.187401
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.000000
0.116802
13.713304
0.000000
0.628526
0.038463
0.016731
0.000000
0.000000
0.000000
0.000000
0.000000
Rates
Total
^
.
0.002419
0.000309
0.000000
0.000000
0.000397
0.003113
0.000262
0.000462
0.000046
0.000118
0.032042
0.000010
0.000656
0.003543
.
,
0.112669
0.094001
0.120058
13.884724
0.000259
0.919637
0.039479
0.016971
0.493436
0.379242
0.053182
0.002784
Appendix B-2)
a pump with two seals.
d) Sources 109-1, 98-0, and 20 were sampled twice because THC was not
on 1/21/81
and 1/22/81
*
operating
-------
TABLE 2-3. COMPARISON OF BENZENE CONTENT IN EMISSIONS AND IN LIQUID LINES:
BETHLEHEM STEEL, BETHLEHEM, PENNSYLVANIA
Temp Press Wt % Benzene Source
Line (°F) (psig) in Line ID
Benzolized 80
Wash Oil
175
Secondary 80
Light Oil 80
a)
b)
c)
d)
e)
f)
50
40
35
Weight percent benzene in
Weight percent benzene in
35 ND° 26-Id
27-0d
66-1
0 ND
10 63
20 63
10 63
10 63
20 63
^. _ Vapor
v Vapor
the total leak =
ND denotes no benzene detected, benzene < 1
I denotes inboard seal, 0
DS denotes dilute sample,
68-1
91
121
98-0
109-1
114
115
116
129
139
141
333-0
334-1
a
Wt % Benzene
in Vapor Leak
73 e
46, DS
73
63, DS
77
78
68
64
82
44, DS
O.DS
20, DS
47, DS
68
98
118*
Wt % Benzeneb
in Total Leak
2.0
46.
1.9
0.9
77.
78.
68.
64.
82.
44.
0.
20.
47.
68.
75.
65.
mass emissions of benzene „ ,„„
mass emissions of NMHC
Total mass emissions of
Total mass emissions of
weight percent
denotes outboard seal of a pump with two
NMHC < 100 ppmv
Analysis of benzene and NMHC were performed
on separate instruments
A l.\J\J
benzene ...
NMHC
seals
; this sample
was probably almost pure benzene
-------
SECTION 3
PROCESS DESCRIPTION
The Bethlehem Steel plant at Bethlehem, Pennslyvania operates with a
wash oil absorption system to recover light oil from the coke oven gas. The
crude light oil product is sent to the Sparrow's Point plant for refining.
During the testing period, the coke ovens were producing 3520 tons per
day of coke and 67.4 MMSCFD of coke oven gas. The light oil recovery unit
was recovering 12,678 gallons per day of crude light oil.
The configuration of the wash oil scrubbers in the light oil recovery
section is shown in Figure 3-1. There are two trains of four scrubbers in
series in each train. A third train on standby has two scrubbers. These
standby scrubbers contained no wash oil during the survey and are operated
only when production levels necessitate.
The remainder of the light oil recovery section is shown in Figure 3-2.
The benzolized wash oil streams from scrubbers 3 and 9 are combined in the
number 3 box. The benzolized wash oil is transferred from this box to the
still, where it is steam stripped to separate the light oil from the wash oil.
The light oil vapor from the still goes to the rectifier, where it is split
into two fractions: an overhead stream called secondary or BTX light oil,
and a bottoms stream called primary light oil. Essentially all benzene is
in the secondary light oil. A portion of the light oil vapor from the still
condenses in the line before it reaches the rectifier. This oil, referred
to as intermediate oil, can be sent to the number 3 box to be combined with
the benzolized wash oil; however, the line that does this had not been used
for at least a month prior to testing.
-------
SCRUBBER 14 SCRUBBER 15
(STANDBY} (STANDBY)
SCRUBBERS
SCRUBBER 10 SCRUBBER 11
SCRUBBER 12
SCRUBBER3
r
BENZOUZED
WASH OIL
VA0040
PU0066
VA0048
puooea
/-I/
DE-SENZOUZED'.
WASH OIL
70-2134-1
Coke Oven Gas (not shown) flows counter-current to the wash oil.
Numbers following the letters VA and PU are source ID numbers for
valves,and pumps, respectively, from which fugitive emissions
were detected.
Figure 3-1. Wash oil scrubber configuration at
Bethlehem Steel, Bethlehem, Pennsylvania.
-------
SECOND L.O. (BTX)
OEBENZOLIZED
WASH OIL
COKE BENZOLIZEO
OVEN ' WASH OIL
GAS <•«*>
INTERMEDIATE
OIL
(NOT IN
SERVICE)
I VA0103
I VA0104
RECTIFIER
'
*
T
PRIMARY L.O.
(NON-BTX)
VA0087 VA0120
VA0124
, VA0129
VA0121
1
,/r
c.w.
VA0115 =
VA0116 8
(3
-i
o
z
m
(0
J-^
> — x
VA0108
^•^
PU0098
PU0109
I
SEPARATOR
LOADING
Numbers following the letters VA and PU are source ID numbers for
valves and pumps, respectively, from which fugitive emissions were
detected.
Numbers in parentheses are the weight percent benzene in that line.
The symbol labelled "Scrubber Trains" represents the wash oil
scrubber trains shown in Figure 3-1.
Figure 3-2. Light oil recovery unit at Bethlehem Steel,
Bethlehem, Pennsylvania.
-------
Fugitive emissions testing was to be performed in all areas of the
plant with at least 4 weight percent or more benzene. This included the
benzolized wash oil, still overhead, rectifier overhead, intermediate oil,
and secondary oil line, and the secondary oil storage and loading areas. The
benzolized wash oil line and the exhausters were screened, although they con-
tained less than 4 percent benzene. The exhausters are upstream from the light
oil recovery on the coke oven gas line, and are not shown in Figures 3-1 and
3-2.
-------
SECTION 4
METHODOLOGY
The fugitive emissions testing at the Bethlehem Steel plant in Bethlehem
included both "screening" and "bagging" operations. Screening is a generic
term covering any quick portable method of detecting fugitive emissions. Bag-
ging refers to a quantitative emission measurement achieved by enclosing the
source in a Mylar® shroud and analyzing an equilibrium flow of air through
the enclosure.
4.1 SCREENING PROCEDURES
Screening was done according to the procedures specified in EPA's proposed
Method 21, a copy of which may be found in Appendix A-2. The instrument used
in performing this screening was the Century Systems Organic Vapor Analyzer
(OVA) Model 108. Method 21 requires the results of the screening to be
recorded (as specified in the applicable regulation) only if the leak defini-
tion is met or exceeded. Since this effort was more oriented to standards
development than to regulatory monitoring, the exact screening value was
recorded for all sources.
The screening methods were used to survey every accessible valve and pump,
and a portion of the flanges, on lines handling at least 4 weight percent benzene.
Only one-third of the flanges were screened because of their large population.
Exhausters were also screened, although they are not in the light oil recovery
section of the plant and the coke oven gas they handle contains less than
4 weight percent benzene. Exhausters were included because they can potentially
have high emissions.
10
-------
The survey was conducted on a line-by-line basis with plant flow diagrams
to ensure that no sources were missed and to group sources subject to similar
process conditions. Plant personnel corroborated the identification of process
lines and supplied data that was not otherwise immediately available, such as
the composition and phase of the material in the line.
One source was not screened due to physical inaccessibility, but this
source was recorded to insure that a complete source inventory was obtained.
All leaking valves, pump seals, and exhauster seals were tagged with their
respective ID numbers and were subsequently bagged.
4.2 SAMPLING PROCEDURES
Bagging procedures were carried out according to methods developed in
previous petroleum refinery testing. Before and after a source was sampled, it
was again screened. This time, however, a J.W. Bacharach "TLV Sniffer" (TLV)
was used in addition to the OVA. The OVA uses a flame ionization detector and
has a quick response time that makes it ideal for the initial screening. The
TLV uses a catalytic oxidation detector and has a slower response than the OVA.
The leaking area of the source was completely enclosed in a shroud of
Mylar® plastic to contain any emissions. Mylar® is well suited to this func-
tion, because it does not absorb significant amounts of hydrocarbons and has
a high melting point (250°C). The enclosures were kept as small as possible,
generally less than one cubic foot in volume except for enclosures of exhauster
seals. A small enclosure provided a more effective seal, minimized the time
required to make the enclosure and reach steady-state conditions, and minimized
the condensation of heavy hydrocarbons within the enclosure.
The enclosure was connected to the sampling train shown in Figure 4-1.
The sampling train included a cold trap, a dry gas meter, and a vacuum pump.
The vacuum pump induced a flow of air, plus any fugitive emissions contained
11
-------
MAGNEHELIC
N>
THIS LINE SHOULD
DEASSIIOnr
POSSIBLE
TEMT
COI.OTRAP
(ICEDATII)
LEAKING
VALVE
TRAP
HO MANOMETER
SMALL
DIAPHRAGM
PUMP
FILTER VACUUM PUMP
SAMPLE DAQ
TWO WAY VALVE
Figure 4-1. Sampling train for baggable source of hydrocarbon emissions.
-------
within the enclosure, through the sampling train. A magnehelic connected to
the enclosure with a short piece of latex tubing was used to ensure that a
slight, but measurable, vacuum was maintained within the enclosure. A slight
vacuum prevented fugitive emissions from leaking out of the enclosure.
The cold trap was used to condense water and heavy organics that might
otherwise condense downstream in lines and equipment. This trap consisted
of a 500 ml flask in an ice bath. No condensate was observed at the Bethlehem
plant; however, if an organic condensate were collected, it would be measured,
analyzed, and included in calculating the total leak rate.
Downstream from the cold trap, a dry gas meter measured the volume of
gas that passed through the sampling train. By measuring the volume of gas
during a known period of time, it was possible to calculate the dry gas
flow rate. The gas flow rate could be varied, and the maximum flow rate
achievable was about 2.5 cubic feet per minute. The temperature and pressure
of the gas were measured to allow a conversion to standard conditions.
When sufficient time had passed to allow the system to reach steady-state
(generally, 4 minutes were more than adequate for an enclosure of 1 cubic foot),
a Tedlar® sampling bag was filled from the discharge of the small Teflon®-lined
diaphragm pump. A second Tedlar® bag was filled with a sample of ambient air
near the enclosure. The two samples were then taken to the mobile lab on the
plant grounds for analysis.
Liquid leak rates were estimated by capturing the liquid in a watchglass
and measuring the volume collected over a known period of time. Samples of
each liquid leak and of the liquids from process lines were taken back to the
laboratory for benzene analysis. Sample bottles were filled to the brim to
minimize any vapor overhead space that would allow the benzene in the liquid
sample to become dispersed between two phases.
13
-------
4.3 ANALYTICAL TECHNIQUES
To quantify the VOC emissions from the bagged sources, the concentration
of total hydrocarbon and also that of benzene were determined using gas chroma-
tographic procedures. Primary analysis of fugitive volatile organic compounds
(VOC) was performed on a Byron 301C Total Hydrocarbon Analyzer (THC). The
THC has an upper detection limit of 20,000 ppmv. Dilutions of more concen-
trated samples were made with a 1.5 liter gas-tight syringe.
Methane calibrations were carried out daily on the THC with an 8000 ppmv
methane/air standard. Nonmethane hydrocarbon calibrations were also carried
out daily on the THC with a 713 ppmw NBS propane standard.
Analyses for benzene were performed on a Hewlett Packard 5730A Dual FID
Gas Chromatograph. Dual gas samples were introduced simultaneously onto sepa-
rate columns with a Valco 10 port Hastalloy C multiport valve installed immedi-
ately forward of the GC syringe injection ports. Peak integrations were com-
piled on two Hewlett Packard 3380A electronic integrators. Liquid samples
were analyzed by normal syringe injection techniques using benzene as an ex-
ternal standard.
The columns and conditions used for the benzene analyses are listed
below:
1/8" OD, 2 mm ID, 15 feet, 5% SP-2100/1.75% Benton 34
on 100/120 mesh Supelcoport.
1/8" OD, 2 mm ID, 15 feet, 10% TCEP on 100/120 mesh
Chromosorb P acid washed.
N2 carrier at 30 ml/min.
Isothermal at 110°C.
The instrument was calibrated daily with a 5571 ppmw benzene in air standard.
Single analyses were done simultaneously on the two different columns after
calibration.
14
-------
SECTION 5
QUALITY CONTROL/QUALITY ASSURANCE
5.1 QUALITY CONTROL FOR SCREENING PROCEDURES
Screening at the Bethlehem plant was done with a single Century Systems
Organic Vapor Analyzer (OVA) Model 108 and one J.W. Bacharach Instrument
Company "TLV Sniffer." The corresponding instrument identification numbers
are given below.
Device Type Assigned ID Number
OVA 3
TLV 4
Two quality assurance activities were used for the screening devices:
• calibration checks, and
• repeated screenings
5.1.1 CALIBRATION CHECKS
The OVA and TLV instruments were calibrated in the morning each day before
they were used. Standards of 90 ppmv and 1990 ppmv hexane in air were used
to obtain a two point calibration on the TLV; 7990 ppmv methane in air was
used to calibrate the OVA. Before a recalibration was made each day, the
values obtained from the instrument were recorded. This served two purposes:
• a check for instrument damage or malfunction, and
• a rough check on the stability of the daily calibration.
15
-------
In addition to the high (and low for TLV) standard calibrations, a dilu-
tion probe was occasionally attached to the instrument and another reading
was taken. The probe was set at 10:1 dilution of the high standard concentra-
tion. The calibration data is summarized in Table 5-1.
The calibration checking results do indicate some significant drift. It
should be noted, however, that these readings are taken in the morning before
calibration and not at the close of the screening day. It is likely that most
of the calibration drift occurs due to the overnight shutdown and recharge rather
than during the days screening. The phenomenon of calibration drift over a
shutdown and re-start has been observed in other studies.
5.1.2 REPEATED SCREENINGS
The reproducibility of screening values was investigated by repeated
screenings of three sources. Two valves and one pump seal were selected to
represent a variety of screening values. Each source was screened once in the
morning and once in the afternoon for five days. Screening was performed with
an OVA by the same operator at all times.
The results of the repeated screenings are plotted for each source in
Figures 5-1 through 5-3. Screening values are plotted on a logarithmic scale
against the date of screening. Variability in screening values for each
source probably reflects the variability in the actual leak rate at the source,
as well as the variability in the response of the screening instrument.
5.2 QUALITY CONTROL FOR ANALYTICAL AND SAMPLING PROCEDURES
Quality control procedures were implemented to insure accurate, consis-
tent, and unbiased analytical and sampling techniques during the project.
The procedures discussed in this section include:
blind standards
• accuracy checks
16
-------
TABLE 5-1. CALIBRATION CHECKING OF OVA AND TLV
Date
01/21/81
01/22/81
01/23/81
01/26/81
01/27/81
01/28/81
OVA 3
High Standard, ppmv"
3000
4500
>10,000
5000
9000
4000
Dil Probe, ppmv"
2500
3000
800
800
800
TLV 4 d
Low Standard, ppmv High Standard, ppmv"
2200
3000
360 2300
300 2000
240 1900
Footnotes:
a) OVA calibration standard contained 7990 ppmv methane in air
b) OVA reading with dilution probe should be 800 ppmv
c) TLV low calibration standard contained 90 ppmv hexane in air
d) TLV high calibration standard contained 1990 ppmv hexane in air
-------
LEGEND: X= REPEATED SCREENING DATA POINT
I
1000UO + ,
I
I
I X X
I
100(10 +.X X x X.
I X
I
I
10(10 •»•
s^
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d lo° *
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>-< I
§ I
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en I
< I
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0 +,
I
I
22 23 24 25 26 27 28
DATE, JANUARY 1981
Figure 5-1. Repeated Screenings at Bethlehem Plant for Pump Seal ID #98
-------
LEGEND: X= REPEATED SCREENING DATA POINT
I
+ ,......... .,•••••••••••• ••••••••••••••••••<
I
I
I
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I
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22 23 24 25 26 27 28
DATE, JANUARY 1981
Figure 5-2. Repeated Screenings at Bethlehem Plant for Valve ID #114
-------
LEGEND: X= REPEATED SCREENING DATA POINT
NJ
O
cx
p.
**-s
w
3
KEENING V/
CO
1
i
i
i
i
i
i
i
i
i
i
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i
i
1 X
1
1 x
1
1
1
1
1
1
1
22 23
X
X
X
X X
24 25 26 27 28
DATE, JANUARY 1981
Figure 5-3. Repeated Screenings at Bethlehem Plant for Valve ID #116
-------
5.2.1 BLIND STANDARDS
An 80 percent benzene liquid standard was submitted to the analyst without
divulging the concentration in order to evaluate the accuracy of the gas
chromatographic analysis of liquid leaks and line samples. Table 5-2 indicates
that the measured benzene content was 81 percent.
TABLE 5-2. LIQUID BLIND STANDARD ANALYSIS RESULTS
Standard I.D. Actual Benzene Measured Benzene
(percent) (percent)
PU 11 80 81
In addition to the blind standard material analysis, a portion of liquid
leak and line samples were analyzed by GC/MS to confirm that the amounts of
benzene found by GC were only benzene and were not coeluting compounds.
Analysis of pure benzene and two samples on each of two columns, as depicted
graphically in Figures 5-4 through 5-10, demonstrates that there were no other
compounds present with the same retention time as benzene.
5.2.2 ACCURACY CHECKS
Accuracy checks were used to evaluate the overall accuracy of the sampling
and analysis techniques. It basically involves inducing a known flow rate of
a concentrated calibration gas into the sampling system and taking a bag sample
of the diluted calibration gas at the exit of the system. Analysis of the bag
sample by THC or GC provides data to calculate the measured leak rate. The
induced leak rate is calculated from the flow rate and concentration of the
induced standard gas.
21
-------
FRM 17437 SPECTRUM 56 RETENTION TIME 3.3
L*K&ST 4« 78.0.189.8 77.0. 33.9 61.0, 31.9 53.0. 20.6
LAST 4t 77.0. 33.9 78.0.100.0 79.0. 8.8 80.1. .3
PAGE 1 V • 1.00
100
80
60
40
30
0
too
80
60
40
20
0.
1-
, .1 Hi'!
1
20 4» 6O 80 ' lo'o ' 130 ' 140 ' 160
180 200 220 24O 2SO S80 300 320
Figure 5-4. Mass Spectrum of Pure Benzene on
SP-2100/Bentone Column
22
-------
UORK AREA SPECTRUM FRN 17443 PAGE 1 V • 1.00
LARGST 41 78.0.100.0 SO.O, 41.3 61.0, 36.0 63. O, 33.6
LrtST 4t 73.9. 9.3 76.0, 7.0 77.0, 30.3 78.0,100.0
* 83 -79 -79
LOO
80
60
4O
30
O
LOO
SO
60
40
30.
ll 1 II
30 4« 60 88 100 120 14O 160
' ISfl ' 200 ' 22fl ' 240 ' 260 ' 280 ' 3,6/0, ' 3g(J
Figure 5-5. Mass Spectrum of Liquid Leak From PU-68
on SP-2100/Bentone
23
-------
UOfflC AREA SPECTRUM FKN 17594 PAGE IV* 1.00
I.A.5O3T 4t 7S.0,lQe.O 77.0, 87.7 53.0. 37.3 61.9, 36.1
UW5T -41 77.0, 87.7 78.0,100.0 70.9, 8.5 84.0, 8.7
* 97 -94
100
89
60
40
80
0
100
OA
60
40
£0.
0
.
^
1 1 1
V inn ilUr J ll ..I...JJ. .....iJ'l
30 40 60 80 100 120 140 160
r .Iflfl F fl«0_. ' 320 V 840 ' 360 ' esa ' 36« ' 32«
Figure 5-6. Mass Spectrum of Liquid Leak from PU-68
on TCEP
24
-------
*« SPECTRUM DISPIAV'EDZT *S
.3UL.G-4.3xg/ai
is-TCEP.i00c,asMi.
FRM 17596
1ST SC/POl 1
x* 1.00 v- 1.00
52.e
78.0
TX
Figure 5-7. GC of Liquid Leak from PU-334
on TCEP
25
-------
FRN 17506 SPECTRUM 109 RETENTION TIME 6.3
LARSST 4t 78.0,100.0 77.9, 34.4 69*0, 38.7 51.0, 31.9
LAST 41 79.0* 7. 3 80.0, ,3 94.9, .4 91.0, .3
PAGE 1 V • 1.00
L00
80
60
40
30
0
100
60
40
30.
0
II
•r*^U^!4
1
30 40 60 ""' 80 ' 100 r"iiS ' £&""' '"" 160
' isa ' ?aa ' as'a ' S40 ' S60 r 2ae ' 3«'^ ' 39a
Figure 5-8. Mass Spectrum of Liquid Leak from PU-334
on TCEP
26
-------
FRN 17506 SPECTRUM til RETENTION TIME 6.4
LARGST 4t 78.9,100.0 77.0, 37.0 51.0, 31.6 50.0, 81. a
LAST 41 77.0. 37.0 78.0,100.0 79.0, 7.3 84.0. 1.3
PAGE IV- 1.00
100
80
60
40
£0
0
100
80
60
40,
20.
0
x-
1
£0 49 60 8« 1M 120 140 160
' 180 ' 200 ' 320 ' 240 ' 260 ' 280 ' 300 ' 320
Figure 5-9. Mass Spectrum of Liquid Leak from PU-334
on TCEP
27
-------
FRN 17441 SPECTRUM 83 RETENTION TIME 4.7
LARCST 4t 73.0,100.9 77.0, 3S.4 53.0, 13.3 51.0. 11.4
LAST 4t 78.0. 4.7 77.0, 8S.4 78.0,190.0 79.0, 6.8
PAGE IV- 1.00
100
80
60
40
30
0
100
QO
60
40.
89.
»)
i in j ill i J....mJLipm*»«mtH
1
30 40 69 BO 100 130 140 169
130 ' 200 ' 9S» ' 94(9 ' 988 ' 280 ' 30O ' ^2^
Figure 5-10.
Mass Spectrum of Liquid Leak from PU-334
on SP-2100/Bentone
28
-------
Table 5-3 lists the data from three accuracy tests. The measured leak
rate, induced leak rate, and the percent recovery are shown. The percent
recovery is calculated as follows:
Percent Recovery = lef k rate X 100%
3 Induced leak rate
The average recovery and its standard deviation are 117.2 percent and 7.61
percent respectively.
TABLE 5-3. ACCURACY CHECKS DATA LISTING
Date
01/21/81
01/21/81
01/26/81
Standard
Type
Benzene
Benzene
Benzene
Measured'
Leak Rate
(Ibs/hr)
0.001005
0.0009484
0.0009669
Induced
Leak Rate
(Ibs/hr)
0.000801
0.0008200
0.0008760
Percent
Recovery
125.4
115.7
110.4
Average recovery = 117.2
Standard deviation= 7.61
29-
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
APPENDIX A
CALCULATIONS AND METHODS
A-l Sample Emission Calculations
A-2 EPA Method 21
30
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
A-l Sample Emission Calculations
31
-------
APPENDIX A-l
EMISSION CALCULATIONS
The emission rates can be calculated from the physical measurements
recorded during the operation of the sampling train and with the anlyses
of the hydrocarbon content of the air passing through the sampling train.
The basic equation is :
kx DF(P-AP)M(C -C )
L
460+
where L = Hydrocarbon vapor emission rate, Ib/hr
_6
ki = 2.75x10 (0R-min-mole/SCF-in.Hg-hr-ppmw)
D = Dry gas meter correction factor (dimensionless)
F = Flow rate, cubic feet per minute
P = Ambient atmospheric pressure, in. Hg
AP = Pressure differential between ambient pressure
and pressure at dry gas meter, in. Hg
M = Average molecular weight of gas (essentially
air) passing through dry gas meter, Ib/lb.mole
Q
T = Total hydrocarbon concentration in air passing
through the dry gas meter, ppmw
r
A = Total hydrocarbon concentration in air near the
sampled leak source, ppmw
T = Temperature of gas (air) stream at the dry gas
meter, °F.
The constant kj is a product of several conversion constants:
(520°R) x (60 min/hr) _
6
(379 - ) x (29.92 in. Hg) x (10 ppmw)
mole
32
-------
ki = 2.75 x 10 6(°R-min-mole/SCF-in.Hg-hr-ppraw)
As an example calculation, assume a total hydrocarbon concentration of 19,000
ppmw was measured in the gas stream from a tent around a leaking source in an
ethylene unit. The hydrocarbon would be assumed to be hexane (MW-86). The
following values were recorded during the sampling:
F = 1.5 CFM
P = 29.9 in. Hg
AP = 2.0 in. Hg (at the dry gas meter)
Q
T = 19,000 ppmw
Q
A = 20 ppmw
T = 75°F
and D = 0.95
10 6
Then M = , „ nnn—;—T^¥
19,000 + 10 - 19.000 >
86 29
The vapor emission rate L is then calculated from Equation (A-l)
T (2.75 x 10~6)(0.95)(1.5)(29.9 - 2.0)(29.37X19.000 - 20)
460 + 75
L = 0.114 Ib/hr.
The vapor emission rate of benzene is estimated from the hydrocarbon
emission rate and the concentration data for benzene and non-methane hydro-
carbons. The equation used is:
„ - , (CB ' °AB) (A-2)
C'T-'A)
where B = Benzene vapor emission rate, Ib/hr
Cg = Benzene concentration in air passing through
the dry gas meter, ppmw
C^g = Benzene concentration in air near the sampled
leak source, ppmw.
33
-------
For example, using the previous example with the data:
CB = 15,500 ppmw
CAB = 10 Ppmw
the benzene vapor emission rate is calculated:
B = 0.114 (15,500 - 10)
(19,000 - 20)
B = 0.093 Ib/hr.
The emission rates for liquid leaks are calculated by the equation:
TLLR =7.93 PV (A-3)
t
where TLLR = Total liquid leak rate, Ib/hr
7.93 = Conversion factor from g/.sec to Ib/hr
V = Volume of liquid collected, cc
t = Time of collection, sec
p = Density of sample, g/cc.
For example, 4.0 cc of liquid from a leaking source were captured in 60
seconds, and the liquid was found to have a density of 0.75 g/cc, then:
TLLR = (7.93)(0.75)(4.0)/(60)
TLLR = 0.40 Ib/hr.
The liquid benzene leak rate is:
BLLR = TLLR [Benz.] (A-4)
100
where BLLR = Benzene liquid leak rate
[Benz]= Benzene concentration in liquid, weight percent
For example, if the liquid leak described above was found to have 79 wt per-
cent benzene then:
BLLR = (0.40)(79)/(100)
BLLR - 0.31 Ib/hr.
34
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
A-2 EPA Method 21
35
-------
PROPOSED METHOD 21. DETERMINATION OF VOLATILE ORGANIC COMPOUND LEAKS
1. Applicability and Principle
1.1 Applicability. This method applies to the determination of
volatile organic compound (VOC) leaks from organic process equipment.
These sources include, but are not limited to, valves, flanges and other
connections, pumps and compressors, pressure relief devices, process
drains, open-ended valves, pump and compressor seal system degassing
vents, accumulator vessel vents, and access door seals.
1.2 Principle. A portable instrument is used to detect VOC leaks
"from individual sources. The instrument detector is not specified, but
it must meet the specifications and performance criteria contained in
paragraph 2.1.
2. Apparatus
2.1 Monitoring Instrument. The monitoring instrument shall be as
follows:
2.1.1 Specifications.
a. The VOC instrument detector shall respond to the organic
compounds being processed. Detectors which may meet this requirement
include, but are not limited to, catalytic oxidation, flame ionization,
infrared absorption, and photoionization.
36
-------
b. The instrument shall be intrinsically safe for operation in
explosive atmospheres as defined by the applicable U.S.A. Standards
(e.g., National Electrical Code by the National Fire Prevention Association).
c. The instrument shall be able to measure the leak definition
concentration specified in the regulation.
d. The instrument shall be equipped with a pump so that a
continuous sample is provided to the detector. The nominal sample flow
rate shall be 1-3 liters per minute.
e. The scale of the instrument meter shall be readable to
±5 percent of the specified leak definition concentration.
2.1.2 Performance Criteria. The instrument must meet the
following performance criteria. The defi-nitions and evaluation
procedures for each parameter are given in Section 4.
2.1.2.1 The instrument response time must be 30 seconds or less.
The response time must be determined for the instrument system
configuration to be used during testing, including dilution equipment.
The use of a system with a shorter response time than that specified
will reduce the time required for field component surveys.
2.1.2.2 Calibration Precision: The calibration precision must be
less than or equal to 10 percent of the calibration gas value.
2.1.2.3 Quality Assurance. The instrument shall be subjected to
response time and calibration precision tests prior to being placed in
service. The calibration precision test shall be repeated every
6 months thereafter. If any modification or replacement of the
37
-------
instrument detector is required, the instrument shall be retested and a
new 6 month quality assurance test schedule will apply. The response
time test shall be repeated if any modifications to the sample pumping
system or flow configuration is made that would change the response
time.
2.3 Calibration Gases. The monitoring instrument is calibrated in
terms of parts per million by volume '(ppnw) of the compound specified in
the applicable regulation. The calibration gases required for
monitoring and instrument performance evaluation are a zero gas (air,
3 ppmv VOC) and a calibration gas in air mixture approximately equal to
the leak definition specified in the regulation. If cylinder
calibration gas mixtures are used, they must be analyzed and certified
by the manufacturer to be within ±2 percent accuracy. Calibration gases
may be prepared by the user according to any accepted gaseous standards
preparation procedure that will yield a mixture accurate to within
±2 percent. Alternative calibration gas species may be used-in place of
the calibration compound if a relative response factor for each
instrument is determined so that calibrations with the alternative
species may be expressed as calibration compound equivalents on the
meter readout.
3. Procedures
3.1 Calibration. Assemble and start up the VOC analyzer and
recorder according to the manufacturer's instructions. After the
appropriate warmup period and zero or internal calibration procedure,
introduce the calibration gas into the instrument sample probe. Adjust
the instrument meter readout to correspond to the calibration gas value.
38
-------
If a dilution apparatus is used, calibration must include the instrument
and dilution apparatus assembly. The nominal dilution factor may be
used to establish a scale factor for converting to an undiluted basis.
For example, if a nominal 10:1 dilution apparatus is used, the meter
reading for a 10,000 ppm calibration would be set at 1,000. During
•field surveys, the scale factor of 10 would be used to convert
measurements to an undiluted basis.
3.2 Individual Source Surveys.
3.2.1 Case I - Leak Definition Based on Concentration Value.
Place the probe inlet at the surface of the component interface where
leakage could occur. Move the probe along the interface periphery while
observing the instrument readout. If an increased meter reading is
observed, slowly probe the interface where leakage is indicated until
the maximum meter reading is obtained. Leave the probe inlet at this
maximum reading location for approximately two times the instrument
response time. If the maximum observed meter reading is greater than
the leak definition in the applicable regulation, record and report the
results as specified in the regulation reporting requirements. Examples
of the application of this general technique to specific equipment types
are:
• •
a. Valves—The most common source of leaks from valves is at the
seal between the stem and housing. Place the probe at the interface
where the stem exits the packing gland and sample the stem
circumference. Also, place the probe at the interface of the packing
gland take-up flange seat and sample the periphery. In addition, survey
39
-------
valve housings of multipart assembly at the surface of all interfaces
where leaks can occur.
b. Flanges and Other Connections—For welded flanges, place the
probe at the outer edge of the flange-gasket interface and sample around
the circumference of the flange. Sample other types of nonpermanent
joints (such as threaded connections) with a similar traverse.
c. Pumps and Compressors—Conduct a circumferential traverse at
the outer surface of the pump or compressor shaft and seal interface.
If the source is a rotating shaft, position the probe inlet within one
centimeter of the shaft-seal interface for the survey. If the housing
configuration prevents a complete traverse of the shaft periphery,
sample all accessible portions. Sample all other joints on the pump or
compressor housing where leakage can occur.
d. Pressure Relief Devices—The configuration of most pressure
relief devices prevents sampling at the sealing seat interface. For
those devices equipped with an enclosed extension, or horn, place the
probe inlet at approximately the center of the exhaust area to the
atmosphere for sampling.
e. Process Drains—For open drains, place the probe inlet at
approximately the center of the area open to the atmosphere for
sampling. For covered drains, place the probe at the surface of the
cover interface and conduct a peripheral traverse.
f. Open-Ended Lines or Valves—Place the probe inlet at
approximately the center of the opening to the atmosphere for sampling.
40
-------
g. Seal System Degassing Vents and Accumulator Vents—Place the
probe inlet at approximately the center of the opening to the atmosphere
for sampling.
h. Access Door Seals—Place the probe inlet at the surface of the
door seal interface and conduct a peripheral traverse.
3.2.2 Case II-Leak Definition Based on "No Detectable Emission".
a. Determine the local background concentration around the source
by moving the probe inlet randomly upwind and downwind at distance of
one to two meters from the source. If an interference exists with this
determination due to a nearby emission or leak, the local background
concentration may be determined at distances closer to the source, but
in no case shall the distance be less than 25 centimeters. Note the
background concentration and then move the probe inlet to the surface of
the source and conduct a survey as described in 3.2.1. If a concentration
increase greater than 2 percent of the concentration-based leak definition
is obtained, record and report the results as specified by the regulation.
b. For those cases where the regulation requires a specific device
installation, or that specified vents be ducted or piped to a control
device, the existence of these conditions shall be visually confirmed.
When the regulation also requires that no detectable emissions exist,
visual observations and sampling surveys are required. Examples of this
technique are:
i. Pump or Compressor Seals—If applicable, determine the type
of shaft seal. Perform a survey of the local area ambient VOC
41
-------
concentration and determine if detectable emissions exist as described
in 3.2.2.a.
ii. Seal system degassing vents, accumulator vessel vents,
pressure relief devices—If applicable,, observe whether or not the
applicable ducting or piping exists. Also, determine if any sources
exist in the ducting or piping where emissions could occur prior to the
control device. If the required ducting or piping exists and there are
no sources of where the emissions could be vented to the atmosphere
prior to the control device, then it is presumed that no detectable
emissions are present.
4. Instrument Performance Evaluation Procedures
4.1 Definitions.
4.1.1 Calibration Precision. The difference between the average
VOC concentration indicated by the meter readout for consecutive
repetitions and the known concentration of a test gas mixture.
4.1.2 Response Time. The time interval from a step change in VOC
concentration at the input of the sampling system to the time at which
90 percent of the corresponding final value is reached as displayed on
the instrument readout meter.
4.2 Evaluation Procedures. At the beginning of the instrument
performance evaluation test, assemble and start up the instrument
according to the manufacturer's instructions for recommended warmup
period and preliminary adjustments. If a dilution apparatus is used
during field surveys, the evaluation procedure must be performed on the
instrument-dilution system combination.
42
-------
4.2.1 Calibration Precision Test. Make a total of nine
measurements by alternately using zero gas and the specified calibration
gas. Record the meter readings (example data sheet shwon in Figure 21-
1).
•4.2.2 Response Time Test Procedure. Introduce zero gas into the
instrument sample probe. When the meter reading has stabilized, switch
quickly to the specified calibration gas. Measure the time from
concentration switching to 95 percent of final stable reading. Perform
this test sequence three times and record the results (example data
sheet given in Figure 21-2).
4.3 Calculations. All results are expressed as mean values,
calculated by:
1 n
I = n -l} xi
Where:
x^ » Value of the measurements.
2 = Sum of the individual values.
— = Mean value.
n = Number of data points.
43
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BETHLEHEM STEEL
BETHLEHEM PLANT
APPENDIX B
ORIGINAL DATA SHEETS
B-l Screening Data
B-2 Screening Sheets for Sample Data
B-3 Sample Data
B-4 Analysis Data
B-5 OVA and TLV Calibration Data
B-6 Repeat Screening Data
B-7 Dry Gas Meter Calibration Data
B-8 Accuracy Check Data
44
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
B-l Screening Data
45
-------
TABLE B-l.l. SOURCE TYPE IDENTIFICATION CODES
Source Type
Flange
Process Drain
Open-End Line
Agitator Seal
Relief Valve
Screwed Fitting
Valves
Block valve - gate type
Block valve - globe type
Block valve - plug type
Block valve - ball type
Block valve - butterfly type
Block valve - other types
Control valve - gate type
Control valve - globe type
Control valve - plug type
Control valve - ball type
Control valve - butterfly type
Control valve - other types
On-Line Pump Seals*
Single, mechanical, emission point at seal
Single, mechanical, emission point at vent
Single, mechanical, other emission point
Double, mechanical, emission point at seal
Double, mechanical, emission point at vent
Double, mechanical, other emission point
Source Type
Code
1
2
3
4
5
6
10
11
12
13
14
15
20
21
22
23
24
25
30
31
32
33
34
35
Continued ...
46
-------
TABLE B-l.l. CONTINUED
Source Type
Source Type
Code
Single, packed, emission point at seal
Single, packed, emission point at vent
Single, packed, other emission point
Sealless pumps
Off-Line Pump Seals
Single, mechanical, emission point at seal
Single, mechanical, emission point at vent
Single, mechanical, other emission point
Double, mechanical, emission point at seal
Double, mechanical, emission point at vent
Double, mechanical, other emission point
Single, packed, emission point at seal
Single, packed, emission point at vent
Single, packed, other emission point
Sealless pumps
On-Line Compressor Seals
Single, mechanical, emission point at seal
Single, mechanical, emission point at vent
Single, mechanical, other emission point
.Double, mechanical, emission point at seal
Double,* mechanical, emission point at vent
Double, mechanical, other emission point
Single, packed, emission point at seal
Single, packed, emission point at vent
Single, packed, other emission point
Sealless compressors
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
Continued
47
-------
TABLE B-l.l. CONTINUED
Source Type Source
Code
Off-Line Compressor Seals
Single, mechanical, emission point at seal 60
Single, mechanical; emission point at vent 61
Single, mechanical, other emission point 62
Double, mechanical, emission point at seal 63
Double, mechanical, emission point at vent 64
Double, mechanical, other emission point 65
Single, packed, emission point at seal 66
Single, packed, emission point at vent 67
Single, packed, other emission point 68
Sealless compressors 69
Exhausters
Suction side 70
High pressure side 71
* 0 = outboard seal; I = inboard seal
48
-------
TABLE B-1.2. STREAM IDENTIFICATION CODES
Code Description of Stream (Columns 25-27)
1 Coke oven gas
2 BTX fraction of light oil; Unit 3 refers to this as
Secondary Oil - a convention different from that used at
Unit 2 where secondary oil is the non-BTX fraction of the
light oil
3 Steam and vaporized light oil
7 Benzolized wash oil
9 Condensables from heat exchanger
10 Benzolized wash oil from scrubbers
11 Benzolized wash oil from scrubbers
12 Benzolized wash oil from scrubbers
13 Benzolized wash oil from scrubbers
14 Intermediate oil
15 Water and light oil from condenser
16 Refers to standby scrubbers used depending upon production
levels. These were not in service during the survey period.
Service
1 Gas
2 Light liquid
3 Heavy liquid
Elevation
1 Sources at ground level
2 Sources at one level above ground level
3 Sources at two levels above ground level
49
-------
SCREENING DATA SHEET
s
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Ul
13
20
Process
Unit
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24
Primary
Material
25
28
Secondary
Material
29
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37
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20
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SCREENING DATA SHEET
Screening
Team
8
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Card 1 [s_
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Comment 1
59
Comment 2
61
68
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-------
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Card 1 Of
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Card 1 [s.
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1. Radian Valve/Pump ID #
2. Unit/Process
3. Plant Name fait)feJl&M ^kd] /&?//?..
Mo. Day
4. Date /O!
11
6. Before Tenting
Screening Time 20
(Military Time)
5. Screener's ID \D\
17
7. Before Tenting OVA
Screening Value 21*
TLV Screening Value
JALtDIO
3 1
8. Screener's ID
38
9. After Sampling |/ |5|2|o
Screening Time ^j
(Military Time)
10. After Sampling OVA
Screening Value
TLV Screening
Value
( 1
iTlelo
52
Comment 1
S3
Comment 2
61
84
-------
Card 1 ISICi
i
1. Radian Valve/Pump ID_ #
SCREENING SHEET
FOR SAMPLE DATA
2. Unit/Process
Cokt &?
3. Plant Name
Mo. Day Yr.
4. Date Ifl/
1 1
6. Before Tenting
Screening Time To"
(Military Time)
5. Screener's ID
17
7. Before Tenting OVA
Screening Value
2"*
TLV Screening Value
I I I I \5\0
3 1
8. Screener's ID
38
9. After Sampling [/ |c>?|2 |O
Screening Time
(Military Time)
10. After Sampling OVA
Screening Value
1 1 1
l/lolo
TLV Screening
Value
(Ill
52
Comment 1
59
Comment 2
61
85
-------
RADIAN
Card 1 IsTCI
i
1. Radian Valve/Pump ID
SCREENING SHEET
FOR SAMPLE DATA
2. Unit/Process
3. Plant Name
»/ fe.4hl0.h&Mj&
Mo. Day Yr.
4. Date \O\ / \l\d&\ 71
11
6. Before Tenting / J5|Sp
Screening Time 2o
(Military Time)
7. Before Tenting OVA
Screening Value 2"*
5. Screener's ID
TLV Screening Value
31
8. Screener's ID
38
9. After Sampling
Screening Time
(Military Time)
10. After Sampling OVA
Screening Value
TLV Screening
Value
1 1 1
1 l'7b
sz
Comment 1
59
Comment 2
6 1
86
-------
Card 1 Is I C
SCREENING SHEET
FOR SAMPLE DATA
1. Radian Valve/Pump ID. //
2. Unit/Process r O W '3>P
3. Plant Name
Mo. Day Yr.
4. Date \Ql\2r?\&i
11
6. Before Tenting
Screening Time To"
(Military Time)
5. Screener's ID
17
7. Before Tenting OVA
Screening Value
•I I I I I 1C
TLV Screening Value
31
8. Screener's ID I—L
38
9. After Sampling [ [ [ [
Screening Time i» i
(Military Time)
10. After Sampling OVA
Screening Value 1*5
TLV Screening
Value
I 1 I 1
I
52
Comment 1
Comment 2
59
6 1
335
87
-------
RADIAN
Card 1
SCREENING SHEET
FOR SAMPLE DATA
1. Radian Valve/Pump ID_#
P13 I fittiOl 31313
3. Plant Name
Beth k
L &
2. Unit/Process
Mo. Day Yr.
Date \0\i
1i
6. Before Tenting
Screening Time
(Military Time)
5. Screener's ID
17
7. Before Tenting OVA
Screening Value 2"
! 1 1
'•^Rl
o|o
TLV Screening Value
I I/
3 1
8. Screener's ID
33
9- After Sampling
Screening Time
(Military Time)
10. After Sampling OVA
Screening Value
I l/lol<
TLV Screening
Value
52
Comment 1
59
Comment 2
61
88
-------
RADIAN
Card 1 Is I Cl
i
SCREENING SHEET
FOR SAMPLE DATA
1. Radian Valve/Pump ID #
3 B If Ml 01*31 "3 Wl 2. Unit/Procesafalfc BP
3. Plant Name
S /gg /.
Mo. Day Yr.
4. Date i <3j < fr j? |6| /
5 . Screener ' s ID
11
17
•6. Before Tenting
.Screening Time To"
(Military Time)
7. Before Tenting OVA
Screening Value 21*
1
ITKIololo
TLV Screening Value
I I J|o|Q|o|
31
8. Screener's ID
38
9- After Sampling
Screening Time
(Military Time)
10. After Sampling OVA
Screening Value TiT
TLV Screening
Value
1 I/
lo|o|o|/
Comment 1
59
Comment 2
61
89
-------
RADIAN
Card 1 Is I cl
i
1. Radian Valve/Pump ID
SCREENING SHEET
FOR SAMPLE DATA
OL3lg"IX|o|Q|2l3
2. Unit/Process
3. 'Plant Name
Ql f/) fe />&*
&M. P<3
Mo. Day Yr.
4. Date I fr* &&}& I
6.
Before Tenting
Screening Time
(Military Time)
5. Screener's ID
17
7. Before Tenting OVA
Screening Value 2I*
1 Ilisiololo
TLV Screening Value
olol 1
3 1
8. Screener's ID
38
9. After Sampling \ f\l \O\O
Screening Time m
(Military Time)
10. After Sampling OVA
Screening Value
\4\o\o\n
TLV Screening
Value
f I WlflblQ
52
Comment 1 I
59
Comment 2
6 1
8*
90
-------
RADIAN
Card 1 Is I cl
i
SCREENING SHEET
FOR SAMPLE DATA
1. Radian Valve/Pump ID #'
2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date
q/
11
6. Before Tenting
Screening Time
(Military Time)
5. Screener's ID
17
,7. Before Tenting OVA
I 1-715 lo lolo
Screening Value 2I*
TLV Screening Value
I l/iololol/
3 1
8. Screener's ID
9. After Sampling | l\i
Screening Time i»i
(Military Time)
10. After Sampling OVA
Screening Value
Comment 1
59
I/
TLV Screening
Value
52
Comment 2
si
91
-------
Card 1 Is I cl
i
1. Radian Valve/Pump ID #
SCREENING SHEET
FOR SAMPLE DATA
Oi3 \£\X\O\O\/tf
2. Unit/Process
&.
3. Plant Name
Mo. Day Yr.
4. Date \O\i
11
6. Before Tenting
Screening Time
(Military Time)
5. Screener's ID
1.7
7. Before Tenting OVA
Screening Value
TLV Screening Value
1
/b loloN
3 1
8. Screener's ID
38
9. After Sampling
Screening Time 1,1
(Military Time)
|JT
10. After Sampling OVA
Screening Value
TLV Screening
Value
I \!\C
>k(o
t
Comment 1
59
Comment 2
61
92
-------
SCREENING SHEET
Card 1
1. Radian Valve/Pump IDJ
FOR SAMPLE DATA
2. Unit/Process
3. Plant Name
Steel
Mo. Day Yr.
4. Date
5. Screener's ID
11
n
6. Before Tenting
Screening Time 20
(Military Time)
7. Before Tenting OVA
Screening Value 21f
1 I4J3
10
o
o
TLV Screening Value
I I / lo io
3 1
8. Screener's ID
38
9. After Sampling
Screening Time
(Military Time)
10. After Sampling OVA
Screening Value
1 1
I3lo|o|o
TLV Screening
Value
f I
52
Comment 1
Comment 2
6 1
93
-------
RADIAN
Card 1 IsTcl
i
1. Radian Valve/Pump ID #
3. Plant Name
SCREENING SHEET
FOR SAMPLE DATA
2. Unit/Process
,,&
Mo. Day Yr.
4. Date
11
6. Before Tenting |_/Jg|5|D
Screening Time 20
(Military Time)
5. Screener's ID
17
7. Before Tenting OVA
Screening Value 2I*
TLV Screening Value
3 1
8. Screener's ID ' '
38
9- After Sampling | | [ |
Screening Time i+1
(Military Time)
10. After Sampling OVA
Screening Value
TLV Screening
Value
[III
1
52
Comment 1
S9
Comment 2
61
94
-------
RADIAN
Card 1 Is I G!
i
1. Radian Valve/Pump ID #
SCREENING SHEET
FOR SAMPLE DATA
Q[3\f\^
2. Unit/Process
3. Plant Name
/.'
Mo. Day Yr.
4. Date
11
6. Before Tenting
Screening Time To"
(Military Time)
5. Screener's ID
17
7. Before Tenting OVA
Screening Value 2I*
TLV Screening Value
3 1
17
8. Screener's ID
Ifllfl/i
38
9. After Sampling | 1\(&)(O\O
Screening Time >* i
(Military Time)
10. After Sampling OVA
Screening Value
1 1 1
1 I/ 15
TLV Screening
Value
52
Comment 1 I
59
Comment 2
s i
95
-------
RADIAN
Card 1
SCREENING SHEET
FOR SAMPLE DATA
1. Radian Valve/Pump ID #
0$ \P\0\4\o\3\-7
2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date lOl/
11
6. Before Tenting
Screening Time To"
(Military Time)
5. Screener's ID \D\fwA
17
7. Before Tenting OVA
Screening Value 21*
I 1 1
1 121*
TLV Screening Value
I I I I
3 1
8. Screener's ID
38
9. After Sampling
Screening Time
(Military Time)
10. After Sampling OVA
Screening Value
TLV Screening
Value
(III
52
Comment 1 I
59
Comment 2
61
96
-------
SCREENING SHEET
Card 1
FOR SAMPLE DATA
1. Radian Valve/Pump ID #
2. Unit/Process
OohJL
Plant Name
Mo. Day Yr.
4. Date
l
11
6. Before Tenting
Screening Time To"
(Military Time)
7. Before Tenting OVA
Screening Value ./
5. Screener's ID
8. Screener's ID
38
TLV Screening Value
31
9. After Sampling \', \(Al IS"
Screening Time m
(Military Time)
10. After Sampling OVA
Screening Value
TLV Screening
Value
52
Comment 1
59
Comment 2
61
97
-------
RADIAN
Card 1 IS I cl
i
1. Radian Valve/Pump ID #
3. Plant Name D&Tn It?
SCREENING SHEET
FOR SAMPLE DATA
2. Unit/Process
4. Date
Mo. Day Yr.
|0|/
5. Screener's ID
11
17
6. Before Tenting
Screening Time
(Military Time)
7.- Before Tenting OVA
Screening Value 2I*
MM
|3|0
TLV Screening Value
I I
3 1
8. Screener's ID
38
9. After Sampling [_/ | /
Screening Time m
(Military Time)
10. After Sampling OVA
Screening Value
TLV Screening
Value
Mil
52
Comment 1
59
Comment 2
61
98
-------
RADIAN
Card 1 Ism
i
1. Radian Valve/Pump ID
3. Plant Name
SCREENING SHEET
FOR SAMPLE DATA
\ftu\o\o\b\8
2. Unit/Process
Mo. Day Yr.
4. Date
61 /
11
6. Before Tenting
Screening Time 20
(Military Time)
Screener's ID \D\P\rt
17
7. Before Tenting OVA
I I I I I/15
Screening Value 21*
TLV Screening Value
1 1
1 1,'f/
3 1
8. Screener's ID
10 n* in
38
9. After Sampling | / | / |-A| *:>
Screening Time m
(Military Time)
10. After Sampling OVA | | [ | )/
Screening Value
TLV Screening
Value
( 1
1 It \L
52
Comment 1 I
Comment 2
99
-------
Card 1 \S_
SCREENING SHEET
FOR SAMPLE DATA
1. Radian Valve/Pump ID # \O\3\ Y\A |Q \O I #l£l 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date
0\l 12.18 la/
11
5. Screener's ID jQl
17
6. Before Tenting
Screening Time 2 o
(Military Time)
7. Before Tenting OVA
Screening Value
1 1 1
1 I -k?
TLV Screening Value
3 1
8. Screener's ID I I
38
9. After Sampling
Screening Time
(Military Time)
10. After Sampling OVA
Screening Value
TLV,Screening
Value
52
Comment 1
59
Comment 2
61
100
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
B-3 Sample Data
101
-------
RADIAN
Card I Ills!
i
SAMPLE DATA SHEET
00
1. Radian Valve/Pump ID# l^fXN" I 1 1 I I i 2. Unit/Process
3
3. Plant Namei c,
Mo. Day Yr.
4.
6. Time
1 1
20
(Military Time)
5. Sampler's Initials I
17
7. Cart ID# [H 8. N.B.# 9. Page
10
. Meter //I U?I0II U
25
11. Time #1 1 I I \Q
37
14. Temp #1 °F I \M\
16. Bar. Press., in. Hg.
12. Meter #2
13. Time #2
I I
15. Temp #2 °F
17. AP, in. Hg.
I I 101,
56
18. DGM Correction! 1 M< i£
Factor 61
20. Vol. Org.
Condensate ml
I I I J I
66
19. Meter
21. Coll. time, minutes
71
22. Specific Gravity l^H—I—J
of Organic
Condensate
75
23. Comment I I I J
102
-------
Card I. IllSl
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# FT"- if \[}W\* f\ 1^1 2. Unit/Process v£',
3
3. Plant Name
Mo. Day Yr.
4. Dat,:
6. Time
1 1
5. Sampler's Initials I
17
I II M2j5|
20
(Military Time)
10. Meter #1 lj*H I ^ / 1
7. Cart ID//
12. Meter #2
8. N.B.i
9. Page #
' I
25
11. Time #1
37
13. Time
#2 I I I \lc
14. Temp #1 °F I 1 ^1 ^ I
u 5
16. Bar. Press., in. He.
51
15. Temp #2 °F 1 I.
"8 ______
17. AP, in. Hg. I I I 1 1^ I2-
56
18. DGM Correction] 1 /I • 1 i' 17
Factor
6 1
19. Meter # "7
2U. Vol. Org.
Condensate ml 66
21. Coll. time, minutes
IJ_U
22.
71
Specific Gravity I I I I
of Organic
Condensate
75
23. ComnifTit I 1 I
78
103
-------
RADIAN
Card I. 11 ISl
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID* PTv-lfmfil\ \&fl I 2. Unit/Process /i
3
3. Plant Name
Mo. Day Yr.
4. Dat,
6. Time
1 1
5. Sampler's Initials I
17
1/1 /I 4).
20
7. Cart ID# [7] 8. N.B.#
(Military Time)
10. Meter #1
25
, \t\o\
3T
11. Time #1 1 1 I Ift
37
12. Meter #2
13. Time #2 I l' \/t
14. Temp #1 °F |
15. Temp *2 °F I
16. Bar. Press., in. Hg.
51
18. DGM Correction] I
Factor 61
l\<\b\1\
~17. AP, in. Hg.
19. Meter #
56
20. Vol. Org.
Condensate ml
I I I 1 j
66
21. Coll. time, minutes L_L_L_i6! 22. Specific Gravity I I I
71 of Organic 7S
Condensate
23. Comment I I I I
78
9- Page
104
-------
RADIAN
Card L |1 I Si
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID// ? I il/ I c', I / 1 C\ I 2. Unit/Process
3. Plant Name ,/M!
Mo. Day Yr.
4. Dat,: l/--'l/
11
6. Time
20
(Military Time)
5. Sampler's Initials L I 'I )
17
7. Cart ID# 8. N.B.# 9. Page f
10. Meter //i Ul'/I ^^ I
25
11. Time #1
37
14. Temp #1 °F
12. Meter #2
13. Time #2
, |5
I I
15. Temp #2 °F
/, -^
M <-f
16. Bar. Press., in. He. I^T/I^ W\7\ 17. AP, in. Hg.
I I \\\<\3.
51
56
18.
DGM Correction! ill- I
Factor 6 *
19. Meter #
f Iff 7
20. Vol. Org.
Condensate ml 66
11. Coll. time, minutes [III I 22.
71
Specific Gravity L I I
of Organic 7S
Condensate
23. Comment | 1 [
78
105
-------
RADIAN
Card I II I Si
l
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# |?|.' I * \A\C\I I2J^"J 2. Unit/Process
-V
-
3. Plant Name />-£/-
Mo. Day Yr.
4. Dat.:
11
A T.
6 . Time '/
(Military Time)
5. Sampler's Initials
17
7. Cart ID#
8. N.B.i
9. Page #
10. Meter #1 lJ\-2.\ 11
25
11. Time #1 1 I I
37
14. Temp #1 °F
16. Bar. Press., in. Hg.
51
18.
DGM rnrrprHnnl_j /I M i\ ill
Factor
61
20. Vol. Org.
I 1 . I 1 I
Condensate ml
66
12. Meter #2 \3\3\£\' 15
31
13. Time #2
15. Temp //2 °F
17. AP, in. Hg.
19. Meter
I I I M ' \
56
21. Coll. time, minutes
I I J — L ! 22.
71
Specific Gravity I I 1
of Organic 75
Condensate
23. Comment II I I
78
106
-------
RADIAN
Card
1 ISl
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# PT^ I /I ,4J C I J I I I 4l 2. Unit/Process
3
3. Plant Name .
Mo. Day Yr.
4. Date
6. Time
bi|Ui3Kn
5. Sampler's Initials I
20
7. Cart ID#
17
8. N.B.#
(Military Time)
10
. Meter //.I I 351.?!'
25
12. Meter #2 "Jf &\ *
31
11. Time #1 I I I \O
37
14. Temp #1 °F I 1 "Vfl
16. Bar. Press., in. Hg.
13. Time #2 I I I
15. Temp #2 °F 1 131 (,|
9. Page #
51
17. AP, in. Hg.
I I I/Ml
56
18.
20.
DGM Correction! I / I . !!
Factor
e i
19. Meter //
Vol. Org. I — I — I — I — i
Condensate ml 66
21. Coll. time, minutes
I I I I 22. Specific Gravity I I 1 1
71 nF Oi"cran-i<- 75
of Organic
Condensate
23. Cumnieiit
78
107
-------
RADIAN
Card I.
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# |T|. |\/| /\|J.| j| { |£| 2. Unit/Process
3
3. Plant Name
Mo. Day Yr.
4. Dat,: I/^U \2 I
11
5. Sampler's Initials
17
6. Time
(Military Time)
10. Meter #1
11. Time #1
25
7. Cart ID#
12. Meter #2
13. Time #2 I I 1
8. N.B.#
\H\0\7\ '\
3l
37
14. Temp
#1 °F I
15. Temp #2 °F 1 l3lC-l
1*8
9. Page #
51
16. Bar. Press., in. He. L^lf I- \¥\7\ 17. AP, in. Hg.
19. Meter f
M I \\'\l
18. -DGM CorrectionLjJj_LliJLtl
Factor
61
20. Vol. Org.
Condensate ml
1 1
1 j
66
21. Coll. time, minutes
22.
71
Specific Gravity I 1
of Organic 7S
Condensate
23. Comment I I I I
78
108
-------
Card L
ryr
SAMPLE DATA SHEET
1. Radian Valve/Pump ID// Kl I \,4>4il?l (l( \k\ 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Dat,: EZ53EZ
11
5. Sampler's Initials
17
6. Time
(Military Time)
7> Cart ID# 8. M.B.f _ 9. Page I
10. Meter #1 9l M I 1 / I
12. Meter #2
11. Time //I I I I l«?
37
13. Time #2 I I I
14. Temp #1 °F I \1\L\
15. Temp #2 °F I I I I
16.
18.
51
Bar. Press., in. He. bj?l ( I* 1^1*71 17. Ap, in. Hg.
4
19. Meter # J_
' I ill*
DGM Correction! ill \D \'7\
Factor
61
ZO. Vol. Org
Condensate ml 66
Coll. time, minutes
22.
71
Specific Gravity ill
of Organic
Condensate
7S
23. Comment: | 1
78
109
-------
RADIAN
Card I FlTs
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# Hi : I V\A\0\i I7I&I 2. Unit /Process (
3. Plant Name
Mo. Day Yr.
4. Dat«:
6. Time
11
(Military Time)
5. Sampler's Initials |
7. Cart ID#
17
8. N.B.#
9. Page
10. Meter #1
25
11. Time #1 1 I I m
37
14. Temp #1 °F
16. Bar. Press., in. Hg.
18. DGM nnrrgpcionl I /I
Factor
6 1
20. Vol. Org.
fi A
Condensate ml
12. Meter #2 4| 61 M > \L>
31
13. Time #2 I I I I!
m
15. Temp
f2 °F \ \1\
17. AP, in. Hg.
19. Meter
I I I /I
5 6
21. Coll. time, minutes
71
22. Specific Gravity L I 1 I
of Organic
Condensate
75
23, Comment I I I
78
110
-------
RADIAN
Card I Ills
SAMPLE DATA SHEET
1. Radian Valve/Pump ID// FT 1 v'lAl £1 I 12 I I I 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Dat
6. Time
1 1
20
(Military Time)
25
37
10. Meter //I
11. Time #1
14. Temp #1 °F I \3
16. Bar. Press., in. He.
51
18.
DGM Correction! 1 \l' \ C\f-\
Factor 61
20. Vol. Org.
Condensate ml 6S
5. Sampler's Initials
17
7. Cart ID# 0 8. N.B.# 9. Page #
12. Meter #2 I/It 9] /
13. Time #2 I I I \(a\
15. Temp #2 °F
17. AP, in. Hg.
' 6
' » Ml/ I/ I
56
19. Meter I - I
21. Coll. time, minutes I I I I I 22.
71
Specific Gravity L I 1 I
of Organic
Condensate
75
23. Ci«mnif-rit I I I I
78
111
-------
RADIAN
Card I.
err
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# I~T I f \0\fl |Q |9 I fi 2. Unit/P
—
3. Plant Name
rocess
Mo. Day
4.
6. Time
1 1
5. Sampler's Initials I
17
(Military Time)
7. Cart ID# QJ 8- N.B.I 9. Page I
10
. Meter #1 \4\l\C\
25
11. Time II 1 I I
37
12. Meter #2 \?\4\ 11 '
3 1
13. Time #2 I I I \(ff
14. Temp #1 °F
15
. Temp #2 °F ' 1 3
16. Bar. Press., in. Hg.
a?l?l
6 1
18. DGM noi-rppt-innl ill iD
Factor
20. Vol. Org.
Condensate ml
17. AP, in. Hg.
19. Meter f "7 /
' I M
S
1 1
1 J
66
21. Coll. time, minutes | I 1 1
71
I 22. Specific Gravity II 1
of Organic
Condensate
75
23. Comment I I I I
78
112
-------
RADIAN
Card L
SAMPLE DATA SHEET
1. Radian Valve/Pump ID// Ml" I Pit/ I 01 MO f\ I 2. Unit/Process j<.'/'
3. Plant Name
Mo. Day Yr.
4. Datf
6. Time
11
/I/..I
20
(Military Time)
5. Sampler's Initials | L
17
7. Cart ID# Q] 8. N.B.# 9. Page
10. Meter #1
25
11. Time #1
37
14. Temp #1 °F I
12. Meter #2
13. Time #2 I I I I
m
15. Temp #2 °F I I
16. Bar. Press., in. Hg.
51
Factor
61
20.
Vol. Org. I—I—I—I—L
Condensate ml 66
17. AP, in. He.
1
I/Ml
56
18. DGM Correction! I / I • 101 M 19. Meter
21. Coll. time, minutes | I I I
71
22. Specific Gravity III
of Organic
Condensate
75
23. Cbnmifnt I [ |
78
113
-------
RADIAN
Card L ills!
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# I 'I" I \f\fl\0 \( |3|7l 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Dat.: 1° I M -I ^KlZ
11
6. Time
(Militay Time)
10. Meter #1 l"7l ' \ $\ > it
25
11. Time #1
14. Temp
#1 °F i
16. Bar. Press., in. Hg.
51
18.
DGM Correction]_iilL_lilLlJ
Factor 6 x
20. Vol. Org.
Condensate ml
rrr.
66
21. Coll. time, minutes
71
5. Sampler's Initials I I ft B\
17
7. Cart ID*
12. Meter #2
13. Time #2 III
8. N.B.#
9. Page
Z
15. Temp #2 °F
17. AP, in. Hg.
19. Meter // 7 /
I I M h I
56
22.
Specific Gravity I —
of Organic 75
Condensate
23. Comment I I I I
78
114
-------
Card L II I Si
i
SAMPLE DATA SHEET
O
1. Radian Valve/Pump ID# fv I" I i/|ff i JEl.^fl^il j 2. Unit/Process /ffiff
3. Plant Name
Mo. Day Yr.
4. Dat,
6. Time
11
(Military Time)
5. Sampler's Initials 1 IJ
17
7. Cart IDI I/J 8. N.B.f
9. Page #
10. Meter //i Rl^ll I'• 1 4 fl 12. Meter #2 \3\t\ '&
25 31
11. Time //I I I I
37
14. Temp #1 °F
16. Bar. Press., in. Hg.
51
18.
DGM Correction! I/ I- \d I?
Factor 6 J
20. Vol. Org.
Condensate ml 66
13. Time #2
15. Temp #2 °F 1 131
17. AP, in. Hg.
1 1
\<\i
56
19. Meter
21. Coll. time, minutes | I I I I 22.
71
Specific Gravity L I I
of Organic
Condensate
75
23. Ci'irauerit I I I I
78
115
-------
RADIAN
Card L Ills!
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID* rT-"'l M 161 I | I Hi \\ 2. Unit/Process /^
3. Plant Name j
-!^
Mo. Day Yr.
4. Dat<:
6. Time
11
5. Sampler's Initials
n
20
7. Cart ID*
8. N.B.*
9. Page *
(Military Time)
10
. Meter *i nT?lOl. I/JPI 12. Meter #2
25
- tf\0\
11. Time #1
13. Time
#2 I I I
37
14. Temp *1 °F
45
15. Temp #2 °F 1 I'.
51
16. Bar. Pressl, in. Hg. I-JUM •• l£ I3l 17. AP, in. Hg.
*
19. Meter * ^7
I I
56
18. DGM CorrectionLJ_/J_jJLa
Factor
I 4 £ 7
61
2.0. Vol. Org.
Condensate ml
I I I I 1
66
21. Coll. time, minutes
22.
71
Specific Gravity L 1 1
of Organic 7S
Condensate
23. Comment III!
78
116
-------
RADIAN
Card L 1
SAMPLE DATA SHEET
A
1. Radian Valve/Pump ID# I I -l\/l/llOl / \QM\ 2. Unit/Process U&,
3. Plant Name
Mo. Day Yr.
A. Dat<
6 . Time
11,
20
(Military Time)
10. Meter //I
11. Time #1
I'll
25
I I lO
37
14. Temp #1 °F
it 5
5. Sampler's Initials I \A ifr |
17
7. Cart ID# 8. N.B.# _ 9. Page //
12. Meter #2 \$\4
13. Time
#2 I I I
15. Temp #2 °F
16. Bar. Press., in. He. I 3JC\I . \^>\5 I 17. AP, in. Hg.
1
UN*
56
18. DGM Correction! I il , I Pi? I
Factor
6 1
19. Meter
ZO. Vol. Org.
Condensate ml 66
21. Coll. time, minutes I I I I I
71
22. Specific Gravity L I 1
of Organic 75
Condensate
23.
78
117
-------
RADIAN
Card L rim SAMPLE DATA SHEET
1. Radian Valve/Pump ID# I~T- I
3. Plant Name /
2. Unit/Process
Mo. Day Yr.
4. Dat,:
6. Time
1 1
5. Sampler's Initials |
20
7. Cart ID#
17
8. N.B.#
(Military Time)
10. Meter //i IfflWl-
25
12. Meter #2 i
11. Time #1 I I I i m
37
13. Time #2 I i I
14. Temp 11 °F
15. Temp #2 °F 1
16. Bar. Press., in. He. I.^Ml « ^131 17. AP, in. Hg.
56
18. DGM CorrectionLjJjL-i^llJ
Factor
19. Meter
6 1
20. Vol. Org.
fi fi
Condensate ml
21. Coll. time, minutes |_L_L_L I 22.
71
Specific Gravity I
of Organic
Condensate
75
23. Comment I I I
78
9. Page
118
-------
RADIAN
Card I II
D
SAMPLE DATA SHEET
i
1. Radian Valve/Pump ID// FT: | \/\ A \ D \ \\ 0\~> \ 2. Unit/P
rocess
3. Plant
Mo. Day Yr.
4. Date
6. Time
11
20
(Military Time)
5. Sampler's Initials I
7. Cart
17
8. N.B.#
9. Page #
10. Meter 11
11. Time #1
37
14. Temp #1 °F I
|0|Q
16. Bar. Press., in. He.\^\ II » I
s i
18.
DGM Correction! 1 / I- I Cl'
Factor
6 1
20. Vol. Org
Condensate ml 66
12. Meter #2
13
. Time #2 I I I l-5i
15. Temp #2 °F L_L
17. AP, in. Hg.
I I Nl7l5l
56
19- Meter
21. Coll. time, minutes
JJLD
71
22. Specific Gravity I I 1I
of Organic
Condensate
75
23. CumniPiit | 1 L
78
119
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# 0\3
3. Plant Name
2. Unit/Process
4. Date
Ho. Day Yr.
o
11
6. Time (Military) | / |/ | 4|
9. Instrument
20
5. Analyst's Initials
7. N.B. f
17
j
8. Page
24
AMBIENT AIR
Component Code
ppnnj
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
37
55
73
ppn&r
23
41
6.
\0\0\l
47
50
Remarks:
120
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1
1. Radian Valve/Pump ID#
3. Plant Name
Mo. Dav Yr.
4. Date
11
9. Instrument
//P-& C/ B*fr
24
2. Unit/Process
5. Analyst's Initials
1. N.B.
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
37
55
73
ppmw
171510
ppinw
23
41
56
59
Remarks:
121
-------
ANALYSIS DATA SHEET
(AMBIENT AMP BAG)
1
1. Radian Valve/Pump ID* |0|3 \£\ X \0 \O \2. \p] 2. Unit/Process Co/it,
3
3. Plant Name
Mo. Day Y'r.
4. Date
0\l
al?
*!/
11
5. Analyst's Initials \^T\
6. Time (Military) / \9 \3\0
7. N.B.
9. Instrument
20
17
8. Page
D
24
AMBIENT AIR
Component Code
pprow
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
47
Remarks:
37
I \6\4\f\°
55
73
pproj
23
41
59
l\0\0\0\0
122
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# 0 1.3 I P I t
3. Plant Name
Mo. Day Tr.
4. Dace
0\l
11
6. Tine (Military)
9. Instrument
20
iflgfe-
g
2. Unit/Process
5. Analyst's Initials \3*\F \&
7. N.B.
17
8. Page
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
47
Remarks:
37
|3|V|0
55
73
ppp&y
23
41
59
\7\0
123
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID// \Q |'3|ff|A&l &\&\£.\7] 2. Unit/Process
. Plant Name
Mo. Day Yr.
4. Date
11
6. Time (Military)
20
9. Instrument
tf?/6C-
5. Analyst's Initials
7. N.B. //
17
8. Page
AMBIENT AIR
Component Code
BAG SAMPLE
Component Code
1."
2.
3.
Card
Comix
4.
5.
6.
0\\ |2-
25
9 *? ?
iQi f , ^—
43
1 1
61
2
ment
2 | A
1
Code
I 1
11
1 1
29
*t\f \°l
Dt
I 1 1 I 15
28
1 1 1 1/10
46
1 1 1 I 1
64
iplicate columns 3
ppmv
1 1 1 1 1
14
1 1 1 I 1 _
32
1 I 1 !/-!/$
through 10 1
Comi
<9M|2-
34
f\3\¥
52
i 1
70
from Card 1
>onent Code
1 1
20
1 1
38
?\f\?
\ 1 1 \$\7
37
1 1 1 |3|6
55
1 I 1 1 1
73
ppnw
1 1 1 1 I
23
1 1 1 1 1
41
\ \ \ \2\0
47
Remarks:
50
56
59
124
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump
3. Plant Name
2. Unit/Process
Mo. Da
4. Date 0\l 2-\
11
6. Time (Military)
9. Instrument /T/yvzX
7 Yr.
7 %\l 5. Analyst's Initials \3\Ffi
17
1 \6\tJ-\0 7. N.B. # 8. Page I
20
C — Oyv^ \ \
T4
AMBIENT AIR
ConroonenC Code
ppmw
BAG SAMPLE
Component Code
37
55
Iff
73
ppmw
23
41
1 1 I
l^l3
59
Remarks:
125
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# 01 3 I Pi Ul 0] 0\ (r, \$
2. Unit/Process
3. Plant Name
4. Date
Mo. Day Tr.
8V
11
6. Time (Military) / 13 I / |5*
9. Instrument/'yCJC
20
5. Analyst's Initials
7. N.B. I
17
8. Page
24
AMBIENT AIR
Component Code
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
\l\°l
37
55
73
ppnw
23
41
6.
Remarks:
1 1
I-Z-IZ
59
126
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID#
3. Plant Name
2. Unit/Process
Mo. Day Yr.
4. Date
0\l oi
11
t
6. Time (Military)
9. Instrument nt /&,
/
* *i /
/I3|3|
5. Analyst's Initials -^fj /
17
0 7. N.B. # 8. Page
?
20
/
24
AMBIENT AIR
Component Code
pprow
BAG SAMPLE
Component Code
Duplicate columns 3 through 10 from Card 1
117
37
55
73
ppnw
23
41
47
Remarks:
50
59
127
-------
6 3 Vfl
54%
U
Sdrx— (U--V, ^f
r >
4 , /
m z
> 0
PU...OO
N.
63 P U f>o7
\
6
—-^—
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
B-4 Analysis Data
129
-------
TABLE B-4.1 COMPONENT CODES FOR ANALYSIS DATA SHEETS
Code Component
001 Methane
012 Benzene
888 OVA reading for sample bag
997 Hexane
998 Non-methane HC
999 OVA reading for ambient air bag
130
-------
1. Radian Valve/Pump ID#
3. Plant Name
Mo. Day Yr.
4. Date
o\\
2-1 1
*!/
11
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
9. Instrument
2. Unit/Process
5. Analyst's Initials
ry) / I C*\l\7
7. N.B.
17
8. Page
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
ppmw
37
73
ppmw
23
41
no
59
Remarks:
131
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# \O\ 3 | ff | k \'0\ &\<9 \ %\ 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date
0\\
il
6. Time (Military) | / | / |/ \O
9. Instrument
20
17
8. Page
5. Analyst's Initials OT^ £
7. N.B. f
5
AMBIENT AIR
Component Code
BAG SAMPLE
Component Code
1.
2.
3.
Card
Compc
4.
5.
6.
^L/l2^
25
1 1
43
1 !
61
2
merit
1 1 1 I 10
28
1 1 1 1
46
1 1 1 1 1
64
2 | A j Duplicate columns 3
1
Code
! 1
11
1 1
29
fl*t^
PpTOV
1 1 1 1 1
14
1 1 1 1 1
32
1 1 l/l»l
0
*
through 10 i
Corat
0\! \2~
34
! 1 _
52
! 1
70
from Card 1
jonent Code
1 1
20
1 1
3jW
9rrrr
" C£.
•••Hit
I l?l7iS*|3
37
! 1 II
55
II II
73
ppnEj
1 1 1 1 1
23
II II
41
CQ
50
Remarks:
132
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1
1. Radian Valve/Pump
3. Plant Name
2. Unit/Process
4. Date
Mo. Day Yr.
Q\\ \^2\*\l
11
5. Analyst's Initials
7. N.B. #
17
8. Page
9. Instrument
AMBIENT AIR
Component Code
BAG SAMPLE
Component Code
1.
2.
3.
Card
Compc
4.
5.
6.
0\l |2-
25
1 1
43
1 1
61
2 2 | A
1
jnent Code
1 1
11
1 1
29
&'?i^-
0 \V
Di
1 1 1 1 \O
28
Mill
46
1 1 1 1 1
64
jplicate columns 3
ppmw
1 1 1 1 1
14
1 1 1 1 1
32
1 \5\6\oV
*
through 10 i
Com]
O( n 2
34
1 1
52
1 1
70
from Card 1
jonent Code
1 1
20
1 1
38
C? u O
7\ W
\
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# |<2|3|v IA \D\/ \O$\ 2. Unit/Process
3. Plant Name
Mo. Dav Yr.
4. Date
o
11
6. Time (Military) / \ty\0 \O
9. Instrument
20
5. Analyst's Initials
7. N.B. #
17
8. Page
AMBIENT AIR
Component Code
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
I I I I \C
37
55
73
23
41
1 1
1 \*\o
47
Remarks:
59
134
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID#
2. Unit/Process
3. Plant Name
Mo. Day
4. Date O\ / 2-|Z
11
6. Time (Military)
"T
9. Instrument r
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump- ID# 0 |3 |v JA |O I I I / I
3. Plant Name
4. Date
Mo. Day Yr.
11
6. Time (Military) / \^j \Z-\0
9. Instrument
20
2. Unit/Process
5. Analyst's Initials
7. N.B.
17
_._ 8. Page
AMBIENT AIR
Component Code
pptnw
BAG SAMPLE
Component Code
Card 2 2 |A Duplicate columns 3 through 10 from Card 1
47
Remarks:
\2\3\l
37
55
73
23
41
59
ppmw
/ |3|0
136
-------
I. Radian Valve/Pump ID#
3. Plant Name
4. Date
Mo. Day Yr.
11
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
. Time (Military)
9. Ins trument///%C — By.*
24
2. Unit/Process
5. Analyst's Initials
7. N.B.
17
8. Page
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
Card 2 2 | A Duplicate columns 3 through 10 from Card 1
47
Remarks:
50
37
55
73
23
41
59
137
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# O\3 I V I A | O| / [/ 15"
3. Plant Name
4. Date
Mo. Day Y'r.
o\i
2)3
*!/
11
6. Time (Military) / \£>\Q\O
20
9. Instrument
\\\[&C
2. Unit/Process
5. Analyst's Initials
7. N.B.
17
8. Page #_
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
5.
6.
47
Remarks:
138
EH??*
37
?! 9
55
73
ppmw
I I I
23
41
59
J nTl
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# |0|3 I V I A \0 \ \ \7-\\ \ 2. Unit/Process L
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# 0 g> |v |A |0| l|2-tf | 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date Oil ^H ^ ^ 1 t'
11
6. Time (Military) /l-^T^l^
20
9. Instrument /fr
25
9\
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# 0 |3|^ | feLl 0\ 0\ 9 I fr 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date
o\\
-2(3
SV
11
6. Time (Military) / \(a \3\O
20
Wkr-
5. Analyst's Initials.
7. N.B. #
17
8. Page
9. Instrument
V
g-
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
)
37
55
73
ppmw
23
41
59
\Z\7\0\0
Remarks:
141
-------
ANALYSIS DATA SHEET
1| A
1
1. Radian Valve/Pump ID#
(AMBIENT AND BAG)
-r
/* /i
^)!3!R JClOl/ltfl? 2. Unit/Process Cc^
fojJ? (A m -7tC*
Mo. Day Tr.
4. Date 0\ / Z| 3 $1 /
11
6. Time (Military) / j7
5. Analyst's Initial
O\0 1. N.B. # 8
. J^nz
17
. Page #
20
9. Instrument n/A/^- / P*#l
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID* 0\?>\ V I A \Q\ \\7)\Cf
2. Unit/Process
3. Plant Name
4. Date
Mo. Day Yr.
0 \ (
11
6. Time (Military)
/ 101510
5. Analyst's Initials
7. N.B. f
17
8. Page
20
9. Instrument /r///?£- ~
24
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
37
1 1
1 I/I?
55
73
ppnw
23
47
Remarks:
50
41
59
I I I I I
13-13
143
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID* 0 \3 \ V | A I 0 I / |Z- |9
2. Unit/Process
3. Plane Name
Mo. Day Yr.
4. Date
0\l
2|6
r|i
11
5. Analyst's Initials \3~\ P\B>
6. Time (Military) / | / | 2- \O
7. N.B.
20
17
8. Page
9. Instrument
5
AMBIENT AIR
Component Code
1.
pprov
BAG SAMPLE
Component Code
64
Card 2 2 | A Duplicate columns 3 through 10 from Card 1
28
46
14
32
50
37
\S\T'
55
73
ppmw
23
41-
59
Remarks:
144
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump IW O\ 3 I V I A \Q I / |4 I I 2. Unit/Process
3. Plane Name
4. Date
Mo. Day Yr.
11
6. Time (Military)
9. Instrument
5. Analyst's Initials \J~\p' \&
17
7. N.B.
8. Page
AMBIENT AIR
c
Component Code
pprow
BAG SAMPLE
Component Code
ppmw
1.
2.
3.
Card
Corapc
4.
5.
6.
0\\
iz-
25
fll
Iff
43
1 1
61
2
jnent
2|A
1
Code
1 1
11
1 1
29
*|?
\°l
Di
1 1 1 \*t\0
28
1 I 1 \5\C)
46
1 1 1 1 1
64
iplicate columns 3
ppmw
1 1 1 1 I
14
1 1 1 I 1
32
1 ! 1 I4P-
«
through 10 i
Conn
6\l 1^
34
^If 1^
52
1 1
70
from Card 1
xment Code
1 1
20
1 I
38
81*|8
1 |Z|3 j5"[/
37
| ,3|^j^|O
55
1 1 1 1 1
73
ppmw
1 1 1 1 1
23
I 1 1 1 1
41
| | \V\0\C
47
Remarks:
50
56
59
145
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# 0 |3 | V | A I 0 I / 10 14
2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date
o\\
11
6, Time (Military) / \(? \O \O
5. Analyst's Initials
7. N.B. #
20
9. Ins trument
AMBIENT AIR
Component Code
BAG SAMPLE
Component Code
jpraw
1.
2.
3.
Card
Compc
4.
5.
6.
#11 12-
25
?tf \%
43
1 1
61
2
jnent
2|A
1
Code
1 1
11
1 1
29
Ml?
Di
1 1 II |3
28
Mill?
46
1 II II
64
iplicate columns 3
ppmv
Mill
14
1 M 1 I
32
II i 1 1 12-
*
through 10 i
Com
6| / |Z
34
9\9 \%
52
1 1
70
from Card 1
>onent Code
1 1
20
1 1
38
SWlS
i II \3\s-
37
1 i I \C\o
55
Mill
73
ppnw
Mill
23
Mill
41
1 II I-Z 1^
50
56
59
Remarks:
146
-------
1. Radian Valve/Pump ID#
3. Plant Name
4. Date
Mo. Pay Y'r.
0\-(
11
6. Time (Military) /| ji| 3
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
lvUlOl/|Q|3
2. Unit/Process
5. Analyst's Initials
7. N.B.
20
17
8. Page
9. Instrument
n/66 —
j
24
AMBIENT AIR
Component Code
pprow
BAG SAMPLE
Component Code
Card 2 2 I A Duplicate columns 3 through 10 from Card 1
1 1
1 1/15-
37
I i I \3\£"
55
73
ppmw
23
41
20
47
59
Remarks:
147
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# \0\2 \ V | A ID \Q\ *?| I 2. Unit/Process
3 '
f\ I/] S~ I
3. Plant Name
4. Date
Mo. Day Yr.
11
6. Time (Military)
9. Instrument
&
b\Qtt
Q
5. Analyst's Initials U\f^\P
7. N.B.
17
8. Page
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
47
50
56
ppmw
I 1 Ui7
/
37
I3i5ir
55
73
ppmw
23
41
59
Remarks:
148
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# 0 |2 I V I A I 0\0\ $\1\ 2. Unit/Process
3. Plant Name
4. Date
Mo. Day Y'f.
o\ \
11
6. Time (Military)
9. Instrument
5. Analyst's Initials
7. N.B. #
17
8. Page
24
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
/|6
37
55
73
ppmw
23
47
Remarks:
50
41
59
7W
149
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID* 0 \ 3 I V U \Q\O]'5\tj
2. Unit/Process
. Plant Name
4. Date
Mo. Day Yr.
11
6. Time (Military) / |7| / I /
20
17
8. Page
5. Analyst's Initials ^IF^P
7. N.B. *
9. Instrument
5
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
ppmw
1710
28
46
64
Card 2 2 j A | Duplicate columns 3 through 10 from Card 1
1
ppmv
14
32
6.
Remarks:
1 1 1
\y\o
50
55
73
ppnw
23
41
59
/in
150
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID# Q\J \V
|3
2. Unit/Process
Gja
3. Plant Name
4. Date
Mo. Day Yr.
11
2-
6. Time (Military)
9. Instrument
01?
20
5. Analyst's Initials \T\F\
7. N.B. I
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
jpmw •
13
37
13 Z\0 M
55
73
ppmw
23
41
56
110 0 0
59
Remarks:
151
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Bump ID# | O\3 \ 9 \ Ml'^l 3 |3 |4 \ 2. Unit/Process
3. Plant Name
4. Date
Mo. Day Yr.
11
5. Analyst's Initials lf\F\£>
17
6. Time (Military)
9. Instrument
\o\o\°
7. N.B.
8. Page //
24
AMBIENT AIR
Component Code
ppmw
/m?
28
46
J I I I I
64
BAG SAMPLE
Component Code
Card 2 2 | A Duplicate columns 3 through 10 from Card 1
ppmw
14
32
I 1 I/
I/
\°
50
Remarks:
152
37
C\I \f\V\c\o\
55
73
ppnw
23
41
59
\l\o\o\o
-------
RADIAN
Card L
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# [ ' I''- 1 /Ml 010
3
3. Plant Name fyjL
2. Unit/Process
Mo. Day Yr.
4. Daf
6. Time
1 1
5. Sampler's Initials I
17
Olftl
20
7. Cart ID#
(Military Time)
10. Meter #1
25
12. Meter 12 H t
11. Time #1 I I I I
37
13. Time #2 1 I t
14. Temp #1 °F
15. Temp #2 °F
1*8
16. Bar. Press., in. Hg. L
51
17. AP, in. Hg.
8. N.B.# 9. Page f
I I
56
18.
DGM Correction! I ? |7 \ Qtf
Factor 61
19. Meter #
20. Vol. Org.
Condensate ml 66
21. Coll. time, minutes
71
22. Specific Gravity L I 1 I
of Organic
Condensate
75
23. Comment
78
153
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
B-5 OVA and TLV Calibration Data
154
-------
UNIT
CALIBRATION CHECKING FORM
.0
*J
a
, «
Pi/
Oil
O\l.
C\l
D\l
o\t
0\l
°\'
0\l
O\l
0\l
^
, s
.ai/
2|Z
2|2
^|3
al^
2|c,
^ |t»
2 |6
-2|6
J|-7
a\-7
Instrument
o
3
**>
\
xj
r
3
4
3
4
?
•V
3
-v
^
Screening
Team
0|/
C'l/
C?|/
0|(
0\l
0|/
»u
0|/
<2|/
o\l
o\l
Low standard
ppm calibration
fl"
1 1 1 1 1
1 1 1 1 1
i
III!'!1
riiii
1 1 1 1 1
1 1 1 i 1
1 1 1 3 IU rO
1 1 1 1 1
i I I^IOR
i i i i i
1 1 &\H\0
High standard
ppm calibration
i Z
i i3iciflifl
1 1^1 r^|C?|0
1 iZl'ZJolo
f
1 ".1 1 o| o 1 o| I
1 13 lo lo 1 0
1 l*|o|o|o
1 li|2|0|0
1 i9l^|o|o
| |^|0|0|O
r iVic>iz>io
•' 1 1 'lliolo
Dilution Probe
Calibration
?n
1 1 1 1 1
1 |-3|^|o'|0
1 1 1 1 1
1 I3|o|o|0
"TVl 1 1
1 1 IfiPtO
i i r&r i
1 1 'iSlolo
1 1 1 1 1.
1 -1 l^|0|0
1 1 1 1 1
WiT
tte
<>>
3
3
B>
o
o
5
">
3
3
3
3
Comments:
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
B-6 Repeat Screening Data
156
-------
TABLE 7-2
REPEAT SCREENING FORM
UNIT #3
CM
qi
0,1
0,
on
I?
Wl
Screening
Team
qi
0,1
q
0(1
211
J
CD
.Process
Dnit
0|3
e>|3
o,3
o,3
10
i i
i
i i i i i i
i I
i\
i i
1 1 1 1 \A
it»
i i
i/i/iV
i i• *? 0
M
a
a) a
a a
15
• O O GO
nAi^iOiO'
rlloloib
III 151
i4|0|0p|0
I I I I 151C
1 1 |2P|0|0
1
JfO O O O
u» V *"^ ^•^
I I \-lg-te-
u
a (M
01 0
,,13
KllO
IV
1 41
a a
41 r-l
D Id
25
I llfllololO
DIol
1 1 I/|B|0|D
1 1 1 k^lDIO
I
o o
/ 3 oo
I |-l|8|o|o
1 1 1 1 1510
'
MCN
5 .
a o
V X
u
^ «
U 3
32 8g
1 1 I I-7P
l |5|0
|sto|opp>
1 1 131 -71^10
i
o
1 1 l/-l«|o|o
0 0
Comments:
j£±
SO
SO
45
So
SO
50
LA I /'rc^
^ Cg?0 O
-------
TABLE 7-2
REPEAT SCREENING FORM
0l
ing
Ul
Scre
Team
Comments:
CD
.Process
Dnit
0)
-
10
1 I/I/If
1
1 1 1 1
III!
1 1 1 1
I.I I I
H>
Ul
Screen
Value
1^21 ol old
I I I I 1516
I I I I I I
I I I
I I I I I I
I I I I I I
I I I I I I
I I I I I I
a fe
tie
22
13 i
|3|ST
1 1
1 1
1 1
1 1
1 1
1 1
Nd
VI
Rescreen-
i&g Value
No
1 1 !
Z2. / OO
iM^-f- I
I l l I
II I I
I I I I l
I I I I l
1 1
I 'I l l i
I l l I l
I l l l l
I I I l l
I I I I I I
32 u
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
B-7 Dry Gas Meter Calibration Data
159
-------
ft*
Card I.
SAMPLE DATA SHEET
1. Radian Valv(?/Pump ID// I I I I I I I 1 I 2. Unit/Process
3. Plant Name
Ho. Day Yr.
4. Dat, I I/ 1/4*1*1/
11
5. Sampler's Initials
/T7
6. Time
(Military Time)
10
. Meter//! l7lQl?l,
~
25
11. Time #1
37
12. Meter #2 ffi/ l5T, f?
13. Time #2 I I I 12-
14. Temp #1 °F I
^5
15. Temp #2 °F 1 i |
16. Bar. Press., in. Hg.
51
18.
DGM Correction] /] x I /I/ I 71
Factor
e i
• \O\j \ 17, AP, in. Hg.
19. Meter #
56
20. Vol. Org
Condensate ml 66
21. Coll. time, minutes
"^1 I I T 22. Specific Gravity
71
of Organic
Condensate
75
23.
78
7. Cart ID# 17] 8. N.B.# 9. Page //
71*
I I 1^ .1 T
160
-------
RADIAN
Card I Ills]
SAMPLE DATA SHEET
1
1. Kadiati Valve/Pump ID# I I I I I I I I I 2. Unit/Process
3
3. Plant Name
4.
6. Time
Mo. Day Yr
1^1 /I /
1 1
20
(Military Time)
10. Meter ll \ \6\?\
25
11. Time #1
37
14. Temp
II °F I
ts
16. Bar. Press., in. Hg.
SI
6 1
18. DGM CorrectionLj_/jL_l£lZJ
Factor
ZU. Vol. Org.
Condensate ml
66
5. Sampler's Initials I
17
7. Cart IDl [D 8. N.B.#
12. Meter #2 lgV?)<7l' |S
31
13. Time #2
15. Temp #2 °F
17. AP, in. Hg.
19. Meter //
48
56
21. Coll. time, minutes
-lH-t-4 22.
Specific Gravity
of Organic 7S
Condensate
23.
78
<^> »T
9. Page
161
-------
Ca rd
i Isl
1
SAMPLE DATA SHEET
r
1. Radian Valve/Pump ID// l~l I I I 1 I I I 2. Unit/Process
3. Plant Name
4. Dat,:
6. Time
Mo. Day Yr.
Ml -TV I
1 1
20
(Military Time)
5. Sampler's Initials
17
7. Cart ID#
8. N.B.//
9. Page
10
. Meter #1 I I\£\C1\<
12
. Meter 12 I /pi ?l • \
11. Time #1
37
i ml
14. Temp #1 °F
>t 5
18. DGM Correction! 1 / P I
Factor
2U. Vol. Org.
Condensate ml
6 i
H-r-r-rr
66
13. Time #2 I I
if i
15. Temp #2 °F i
16. Bar. Press., in. He. IcQl °l\ • \7\
51 *
17. AP, in. Hg.
19. Meter //
21. Coll. time, minutes | -I- I - I I
71
22. Specific Gravity I""!
of Organic 75
Condensate
23. Comment I—|—|~ '
78
162
-------
BETHLEHEM STEEL
BETHLEHEM PLANT
B-8 Accuracy Check Data
163
-------
ftf
03\/flOOt\
Card L |1 |S|
i
SAMPLE DATA SHEET
c&r1
_/ss^_.
A\C\l\t
1. Radian Valve/Pump ID# l/(2l /I 7\4'\8\/\l i 2. Unit/Process
3
3. Plant Name
Mo. Day Yr.
4.
6. Time
1 1
5. Sampler's Initials
17
(Military Time)
7. Cart ID#
8. N.B.i
9. Page I
10. Meter #1 \5\Q\6\ .
12. Meter #2 iXt /I5f l/^
11. Time #1
I I
37
13. Time
14. Temp #1 °F
15. Temp #2 °F i I |
16. Bar. Press., in.
• P> I/
17. AP, in. Hg.
18.
DGM Correction] /I / I/ I/ j/ 1 19. Meter #
TTo /-» <- r^-^ ** 1
hrrrT
Factor
2U. Vol. Org.
Condensate ml 66
21. Coll. time, minutes
71
"I I I I " 22. Specific Gravity III!
of Organic
Condensate
75
23.
-------
RADIAN
Card I.
rrra
SAMPLE DATA SHEET
A C o o o I
1. Radian Valve /Pump ID# F#T7 I /I ~*\1 \ fl/T/i 2. Unit/Process
3. Plant Name
/.'/,.,', \77, /'
Mo. Day Yr.
4. Dat,
6. Time
1 1
5. Sampler's Initials I
20
7. Cart ID#
17
8. N.B.#
(Military Time)
9. Page
10. Meter #1 I/ (r 13V H K
25
12. Meter #2 IjJ^ 1Z 1 * 10 lOi 1,1$
3'1
11. Time #1 I I I \n\
37
13. Time #2 I I
14. Temp #1 °F |_1
15. Temp #2 °F
1*8
16. Bar. Press., in. Hg. |3|(DL /)
51
56
18. DGM CorrectionLjJ_L_l£l£J
Factor
17. AP, in. Hg.
19. Meter i J/Sff? 2-
\l\.\!
6 1
20. Vol. Org.
Condensate ml
66
21. Coll. time, minutes
22.
71
75
23. Comment I
78
f^r—r^l
Specific Gravity 11 1 I
of Organic
Condensate
•
.- *
165
-------
Card L 1
s]
SAMPLE DATA SHEET
1 O3ACOOO2.
r
1. Radian Valve/Pump ID#
3. Plant Name
2. Unit/Process
4. Date
6. Tlme
Mo. Day Yr.
5. Sampler's Initials I
17
(Military Time)
7. Cart ID#
8. N.B.i
9- Page
DO, oo
25
10. Meter #1 \j III fl
9 *; »
11. Time #1
12. Meter #2 U I I ll
37
I \0\
13. Time
#2 I I I
14. Temp #1 °F I
15. Temp #2 8F 1 I
16. Bar. Press., in. He. I3IN • M I fc
s i
18.
20.
DGM Correction! 1 /I t \0 l
Factor
61
17. AP, in. Hg.
j
19. ' Meter I 7^/ 3 £
l/l/ 10
Vol. Org.
Condensate ml 66
1—t—i—r-r
21. Coll. time, minutes t' I L
71
22. Specific Gravity \~~\
of Organic
Condensate
75
23. Comment 1—j-
78
*' \
^1' -
s\
,}
-' -
l^yi^I^
166
-------
RADIAN
Card L 11 ISI
i
SAMPLE DATA SHEET
o 3 A c o o o 3
1. Radian Valve/Pump ID# I'/Ht'l I \,1\M V| Mir 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Dat,:
6. Time
1 1
5. Sampler's Initials
17
20
(Military Time)
7. Cart ID# Q] 8. N.B.I 9. Page I
z1*
. Meter #1 161 f l*f|. Hl^l 12. Meter #2
10.
11. Time #1
2 5
I I 10
37
14. Temp #1 °F
^s
13. Time #2 I I I
i»i
15. Temp #2 8F 1 l-l^
16
. Bar. Press., in. Hg. I Al Cf I J^M 17. Ap in. Hg.
51
56
61
18. DGM rnrr«ri"tnnl I /I. lOl7l 19. Meter I ^/_
Factor
20. Vol. Org.
Condensate ml
66
21. Coll. time, minutes
II II 22. Specific Gravity
71
of Organic
Condensate
75
23. Comment I I I I
78
t
*
v
167
-------
RADIAN
• to'
Card I
SAMPLE DATA SHEET
1. Radian Valve?/Pump ID// U\C\ I \.£\ Q I S"l / I / I 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Dat.i l<3l/
1 1
5. Sampler's Initials I li
17
6. Time
(Military Time)
7. Cart ID*
10. Meter //i
11. Time #1
25
I I
37
I 8. N.B.#
12. Meter #2 Iffi^lfl. I ^"51
13. Time #2
9. Page
14. Temp
#1 °F I
16. Bar. Press., in.
18.
DGM Corrertir.nl I II
Factor
15. Temp #2 °F
17. AP, in. Hg.
19. Meter //
56
6 l
ZO. Vol. Org.
Condensate ml 66
21. Coll. time, minutes I II I I 22. Specific Gravity L~~T" ] I
of Organic
Condensate
23. Comment I ~i
78
- n$ s
r^' 4
L
168
.'3
X
-------
RADIAN
Ca rU L 1
SAMPLE DATA SHEET
i
1. Radian Valve/Pump ID// \1\\C\ I \Z\Q !
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
O 3 A c o o a (
1. Radian Valve/Pump IW
3. Plant Name
12. Unit/Process
Sfel
4. Date
Mo. Day Yr.
11
r/
5. Analyst's Initials U\
6. Time (Military) | / | 6 \ 4} 6
20
7. N.B.
T7
8. Page
9. Instrument
HP
24
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
ppmw
1.
2.
3.
Card
Compc
4.
5.
6.
on
1^
25
1
43
I
61
2
jnent
|
2 i A
Di
1
Code
1
11
1
29
I
1 1 1 1 \0
28
1 1 1 1 1
46
III!!
64
iplicate columns 3
ppmw
Mil!
14
1 1 1 1 1
32
MM!
*
through 10 J
Com]
0
34
_J
n*.
I/ |0 |9 1* |"7
37
1
52
1
70
from Card 1
jonent Code
1
20
1 1
38
1 I
MM!
55
I 1 M 1
73
ppnw
M 1 M
23
M 1 M
41
Mil!
47
Remarks:
50
56
59
170
-------
1. Radian Valve/Pump ID# |A 1C. I fi I i I Z I / I ?
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
O3 AGO 002
. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date Oil 2- 1 1 ?! I
11
6. Time (Military) / | / |3 \0
20
9. Instrument Ml/ ^?^ — 2-
J 24
5. Analyst's Initials -Jf^) ^
17
7. N.B. # 8. Page #
AMBIENT AIR
Comoonent Code
ppmw
BAG SAMPLE
Component Code
1.
2.
3.
Card
Compc
4.
5.
6.
0|||^
25
I 1
43
1 1
61
2
ment
2 |A
1
Code
1 1
11
| |
29
1 1
Dt
I 1 1 1 10
28
1 1 1 1 I
46
1 1 1 1 1
64
iplicate columns 3
ppmv
I 1 1 1 1
14
1 1 I I 1
32
III!!
*
through 10 i
Com{
o\\ \i>
34
1 1
52
1
70
from Card 1
jonent Code
1 1
20
1 1
38
I
I \6\i\-\7
37
1 1 1 1 1
55
I 1 1 I 1
73
ppmw
1 1 1 1 1
23
1 1 1 1 1
41
1 1 I 1 1
CO
47
50
Remarks:
171
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
03 A c o o o 3
1. Radian Valve/Pump ID# ?JJC \0
2. Unit/Process
3. Plant Name
4. Date
Mo. Day Yr.
11
<0
6. Time (Military)
9. Instrument
5. Analyst's Initials
7. N.B. I
7
8. Page
24
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
1.
2.
3.
Card
Compc
4.
5.
6.
011
12-
25
1
1
43
|
61
2
snent
2 |A
I I 1 I 10
23
1 1 1 1 1
46
Mill
64
Duplicate columns 3
1
Code
1 1
11
1 1
29
|
ppmv
Mill
14
Mill
32
Mill
*
through 10 i
Conn
o\\ \i~
34
1 1
52
I 1
70
from Card 1
jonent Code
! 1
20
1 1
38
1 !
1 1 L"fl /I/I
37
1 1 I 1 1
55
1 1 1 1 1
73
ppmw
1 1 1 1 1
23
1 I 1 1 1
41
I 1 1 1 1
59
Remarks:
172
-------
)\
g
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1
1. Radian Valve/Pump ID#
2. Unit/Process
. Plant Name
4. Date
Mo. Day Yr.
11
6. Time (Military) /\
9. Instrument
20
5. Analyst's Initials i
24
AMBIENT AIR
Component Code
pprow
BAG SAMPLE
Component Code
1.
2.
3.
Card
Compc
4.
5.
6.
^Sff
25
d( /
z.
43
2
T
ment
?
r
2|A
Dv
1
Code
11
29
71?!?
1 1 1 l-"|6
28
1 1 1 1 \g
46
¥ 1 1 . I 1
1 1 II 1
64 s*~
iplicate columns 3
ppmv
1 1 1 1 1
14
1 1 I 1 1 _
32
1 1 1 1^10
.
••*-
through 10 i
Corai
^l/ 12.
34
.
52
L 1
1
9\9\tf
70
from Card 1
>onent Code
1
20
I
3ft
C?i S? i$?
^r |^ |o
1 1 1 2\6
37
• " ~\ — 1
55
1 £\O
73
ppmw
1 !
23
1 I
41
|2t-sf^P
47
50
56
Remarks:
173
-------
ANALYSIS DATA SHEET
(AMBIENT AND BAG)
1. Radian Valve/Pump ID#
3. Plant Name
7,
2. Unit/Process
<^4
4. Date
Mo. Day Yr.
01
11
5. Analyst's Initials
6. Time (Military)
9. Instrument
20
7. N.B.
8. Page
AMBIENT AIR
Component Code
ppmw
BAG SAMPLE
Component Code
ppmw
1.
2.
3.
Card
Compc
4.
5.
6.
011 IX-
25
nent
2 |A
1
Code
I 1
11
1 1
29
ftffl
Di
1 1 1 I/&I9
28
i 1 1 12I5"
46
1 M 1 1
64
iplicate columns 3
ppmw
M M 1
14
Mill.
32
1 1 1 l^|5"
*
through 10 J
Com]
O\l \2-
34
?[9 jSj
52
1 1
70
:rom Card 1
jonent Code
1 1
20
1 1
38
v\sr\?
\ \ 1/1514
37
1 I 1319 10
55
1 M 1 1
73
ppmw
M M 1
23
Mill
41
1 1 \S\-7\0
47
Remarks:
50
56
59
174
-------
RADIAN
Card L
SAMPLE DATA SHEET
x<
1. Radian Valve/Pump ID# P f- l\/l/h d\0\^\"^\ 2. Unit/Process UK
3
3. Plant Name (/)LJL yul!
Mo. Day Yr.
4. Dat,:
6. Time
11
[Uo\
20
(Military Time)
25
11. Time #1
37
14. Temp #1 °F
r
1 4l
us
16. Bar. Press., in. Hg. u
5 1
18.
DGM CorrectionJ__Lj_L
Factor 6l
20. Vol. Org.
Condensate ml
'1 IT-lL
66
21. Coll. time, minutes
5. Sampler's Initials
17
7. Cart ID#
8. N.B.#
10. Meter //i \fi\M\, \5\0\ 12. Meter #2 Lj_
r i i
71
23. Comment
78
31
13. Time #2 I I I
15. Temp #2 °F 1
17. AP, in. Hg.
56
19. Meter
22. Specific Gravity L
of Organic 75
Condensate
9. Page //
175
-------
Card L
ITTsI
SAMPLE DATA SHEET
___
1. Radian Valve/Pump ID# I M - \f\H iVfl ?\Z\'3l 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date;
6. Time
11
(Military Time)
5. Sampler's Initials I
17
7. Cart ID# Q] 8. N.B.
9. Page
10. Meter
11. Time #1
25
37
14. Temp #1 °F I J 3m
12. Meter #2
13. Time #2 I
i
15. Temp #2 °F 1 I I
16. Bar. Press., in. Hg.
SI
18. DGM Correction! l\<
Factor
6 1
20. Vol. Org. I—I—I—I—L
Condensate ml 66
17. AP in. Hg.
* e
I i I / I <
56
19. Meter #
21. Coll. time, minutes
71
22. Specific Gravity L I 1
of Organic 7S
Condensate
23. Comment
I I
78
176
-------
RADIAN
Card L
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# r I ^\f'\fj \0 \ 3\3\Lf\ 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Dat,:
6. Time
1 1
\CflW
(Military Time)
5. Sampler's Initials I
7. Cart ID#
17
8. N.B.//
9. Page
10
. Meter #1 I _ \6\lt\:
2 5
11. Time #1 'ill
37
14. Temp #1 °F I i
ts
16. Bar. Press., in. Hg.
18. DGM Hnrrercionl 1 /I ' I/?1/H
Factor
61
20. Vol. Org.
Condensate ml
66
21. Coll. time, minutes
12. Meter #2
31
13. Time #2 I I I
41
15. Temp #2 "F 1
1*8
17. AP, in. Hg.
19. Meter
I i I If. 13
56
I| ] | | 22. Specific Gravity 1 I 1 '
71 of Organic
Condensate
75
23. Comment [_ | I J
78
177
-------
RADIAN
Card L
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# I 'I : \f.\X\fi\Q\0-&\ 2. Unit/Process
3. Plant Name
Mo. Day Yr.
4. Date;
6. Time
5. Sampler's Initials I
20
(Military Time)
10. Meter //i
11. Time #1
25
I Jiff]
I I 10
37
7. Cart ID#
12. Meter #2
13. Time #2 I I I
17
8. N.B.#
9. Page
iTI
(
14. Temp #1 °F I
16. Bar. Press., in. He.
' \T~\tf
s i
18. DGM Correction,
Factor
20. Vol. Org.
6 i
ill
15. Temp #2 °F
17. AP, in. Hg.
19. Meter //
56
Condensate ml 66
21. Coll. time, minutes | I I I I 22. Specific Gravity L I I I
of Organic
Condensate
71
75
2 3. Ct>mnie: n t
78
178
-------
RADIAN
Card L 11 Is
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID// p| " | £|Ml> \0\l\T\ 2. Unit/Process
3. Plant Name
Mo. Day
4. Dat,:
6. Time
11
-sat
J*«3C I ^A Jl
5. Sampler' s Initials I W-_l P|
17
7. Cart ID# IT] 8. N.B.#
(Militay Time)
/ I ^ .70
10. Meter #1 I ^
9. Page
12. Meter #2 \I\A\ l\ ' I /I/I
11. Time #1
37
I 101
13. Time #2 III l4-
14. Temp #1 °F I
15 Temp #2 °F 1
/. 3
16
. Bar. Press., in. Hg. l^?l 01 ' I ?l Si 17. AP, in. Hg. Ll
S'l • • 56
18. DGM Correct ionj__jjli_lili3j
Factor 6 x
20. Vol. Org
19. Meter
eg
Condensate ml
21. Coll. time, minutes
71
22. Specific Gravity I\ 1 I
of Organic
Condensate
75
23. Comment | 1 _[..
78
179
-------
Card I. I 1 I Si
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# FT-> I tj )Cj d\ 0( ||f I 2. Unit/Process
3. Plant Name (_
Mo. Day Yr.
4. Dat,:
6. Time
1 1
(Military Time)
5. Sampler's Initials | |_
17
7. Cart ID# [7] 8. N.B.// 9. Page //
zV
10. Meter #1 [j.
25
11. Time #1
I I lO
37
14. Temp #1 °F
12. Meter #2 I] |1 I ^ >l
13. Time #2 I I I
15. Temp 12 °F
16. Bar. Press., in. Hg.
51
18.
DGM Correction] I Jl * iD iTi
Factor
6 1
20. Vol. Org.
I 1 1
J
Condensate ml 66
17. AP, in. Hg.
19. Meter #
56
21. Coll. time, minutes
71
22. Specific Gravity | L
of Organic 75
Condensate
23. Cnmment I I I
78
180
-------
RADIAN
Card I
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# I ' Pl£i)C|/9 \D \2~\0\ 2. Unit/Process
3
3. Plant Name
Mo. Day Yr.
4. Datu
6. Time
11
20
(Military Time)
5. Sampler's Initials |
17
7. Cart ID#
8. N.B.//
9. Page
10. Meter //I UL&7I «• 10-P I 12. Meter #2
11. Time #1
37
14. Temp #1 °F
16. Bar. Press., in. Hg.
S 1
18.
DGM
Factor
6 1
20. Vol. Org.
Condensate ml
13. Time
15. Temp #2 °F I
"48
A\ ft' \1\*
17. AP, in. Hg.
19. Meter #
66
II \\\'V\
9 O
21. Coll. time, minutes
I I I I 22. Specific Gravity I—I 1 '
71 of Oraanic 75
of Organic
Condensate
23. Commont
78
181
-------
RADIAN
Card L
rrra
SAMPLE DATA SHEET
1. Radian Valve/Pump ID# I • I'."- | ^
3. Plant Name
2. Unit/Process
Mo. Day Yr.
4. Date
6. Time
11
(Militay Time)
10. Meter #1 I :lC 1 I I • 1 41C
25
11. Time #1 I I I
37
14. Temp #1 °F L
16. Bar. Press., in. Hg.
5 1
18. DGM Correction! I ll .• I Cl
Factor
e i
20. Vol. Org.
I I I I I
Condensate ml 66
5. Sampler's Initials I
17
7. Cart ID#
8. N.B.i
9. Page #
12. Meter #2 H'f / \C\-\.3tf\
13. Time
#2 I I I I?
15. Temp #2 °F
17. AP, in. Hg.
19. Meter #
"•8
56
21. Coll. time, minutes | I 1 I I
22.
71
Specific Gravity L I I
of Organic
Condensate
75
23. Comment [
78
182
-------
Card L
rrm
SAMPLE DATA SHEET
* 1
a— T..n......i - - - - , £ J *
1. Radian Valve/Pump ID# P I" If- 1J I #1*1 111 I 2. Unit/Process / / fc_'
3. Plant Name :^x
Mo. Day Yr.
4. Datr LL.
11
5. Sampler's Initials i
17
6. Time
(Military Time)
7. Cart ID// I /I 8. N.B.#
10. Meter //i I '5(0 l.3| I
25
12. Meter #2 |3f ?l Vl
11. Time #1
13. Time #2 I I I
37
m
14. Temp *1 °F I 1
16. Bar. Press., in. Hg.
15. Temp #2 °F i I
l~ho
51
18.
DGM Correction]_jJ_L_jLl3j
Factor
17. AP, in. Hg
19. Meter # ^
56
_
6 1
ZO. Vol. Org.
Condensate ml
I I I — I — 1
66
9. Page
21. Coll. time, minutes
22.
71
Specific Gravity I i 1
of Organic 75
Condensate
23. Comment
LL
78
183
-------
RADIAN
Card I
SAMPLE DATA SHEET
1. Kadian Valve/Pump ID# HT-" I 'J '\\^ \Z\ll\Q\ 2. Unit/Process L~£~
w_- ^f-
3. Plant Name ,
Mo. Day Yr.
4. Dat,:
6. Time
1 1
20
(Military Time)
5. Sampler's Initials I I M\
17
7. Cart ID!
8. N.B.I
9. Page
10. Meter #1
25
11. Time #1 I I I
37
14. Temp #1 °F
"iS
16. Bar. Press., in. Hg.
Factor
20. Vol. Org.
61
Condensate ml 66
12. Meter #2
13. Time #2 I I
15. Temp #2 °F 1
17. AP, in. Hg.
18. DGM Correction! ill. lbf?l 19. Meter I
21. Coll. time, minutes
71
22. Specific Gravity L I 1 |
of Organic
Condensate
75
23. Commont L I L
78
184
-------
RADIAN
Card L
SAMPLE DATA SHEET
1. Radian Valve/Pump ID// 1 ' \~ \ ?\i'\-.\^ h'. |6 I 2. Unit/Process /V/fc/
3 ~*
3. Plant Name
- /T///6 _ W<" /
,1
Mo. Day Yr.
4. Dati:
6. Time
11
(Militay Time)
5. Sampler's Initials I 1
17
7. Cart
8. N.B.#
9. Page
10. Meter //I
25
11. Time #1 |_1
37
14. Temp #1 °F I 1
1 3
16.
18.
Bar. Press., in. Hg.
s i
DGM rm-rert-inni I /I • I & I f\
Factor 61
20. Vol. Org.
I I I I ]
Condensate ml
66
12. Meter //2
13. Time #2
3 1"
I I
15. Temp #2 °F 1 1 I
17. AP, in. Hg.
56
19. Meter #
21. Coll. time, minutes
| | L I 22. Specific Gravity L I I
71
of Organic
Condensate
75
23. Cumnierit
185
-------
i i ITT7I
ard L II IS)
SAMPLE DATA SHEET
1. Radian Valve? /Pump ID# I - \".- I
_____^ -
' Ik ffl I 2. Unit/Process (.£&
3. Plant Name
Mo. Day Yr.
4. Dat.:
6> Time
11
MOifl
(Militay Time)
5. Sampler's Initials I 1
17
Cart ID#
. N.B.i?
9. Page
10. Meter #1 kC7l5l.
12. Meter #2 \5\C\k\. \'
11. Time #1 I I I I /M
37
14. Temp #1 °F I
16. Bar. Press., in. He.
II
51
61
20. Vol. Org.
Condensate ml
66
13. Time #2 I I I I
15. Temp #2 °F 1
-a
17. AP, in. Hg.
I \ /\'\v\
56
18. DGM Correction! 1 I I lO iTl 19. Meter
Factor
21. Coll. time, minutes
I I I I 22. Specific Gravity I I I I
71
of Organic
Condensate
75
23. Cumment
78
186
-------
RADIAN
Card L |1 I SJ
i
SAMPLE DATA SHEET
1. Radian Valve/Pump ID// I I I I I I I I I 2. Unit/Process (sl'S
3 *^
3. Plant Name
•'^ /.»' .;-
Mo. Day Yr.
4. Daf: I**!
H
6. Time
?
(Militay Time)
5. Sampler's Initials I t//l7>l
17
7. Cart ID#
8. N.B.#
9. Page
10. Meter //I I I I I 1 I I
25
11. Time #1
37
14. Temp
#1 °F I 1 I 1
16.
18.
Bar. Press., in. Hg.
5 1
1C
DGM Correction]_jJjjJ_LJ_£]
Factor
20. Vol. Org.
Condensate ml
66
12. Meter #2 I I 1 1 I II
13. Time #2 \ I I I
15. Temp #2 °F I I I I
17. AP, in. Hg.
.
56
19- Meter #
21. Coll. time, minutes
71
22. Specific Gravity i_ 1 I 1
of Organic
Condensate
75
23. Comment I 1
78
187
------- |