EPA-670/2-73-082
February                 Environmental Protection Technology Series
New Microbial Indicators
of Wastewater
Chlorination Efficiency
                                 Office of Research and Development
                                 U.S. Environmental Protection Agency
                                 Washington, D.C. 20460

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            RESEARCH REPORTING SERIES
Research reports of the  Office  ot  Research  and
Monitorinq.  Environmental Protection Agency, have
been grouped into five series.  These  five  broad
categories  were established to facilitate further
development  and  application   of   environmental
technology.   Elimination  of traditional grouping
was  consciously  planned  to  foster   technology
transfer   and  a  maximum  interface  in  related
fields.  The five series are:

   1.  Environmental Health Effects Research
   2.  Environmental Protection Technology
   3.  Ecological Research
   14.  Environmental Monitoring
   5.  Socioeconomic Environmental studies

This  report has been assigned to  the ENVIRONMENTAL
PROTECTION  TECHNOLOGY   series.    This    series
describes   research   performed   to   develop   and
demonstrate    instrumentation,     equipment     and
methodology  to   repair   or   prevent environmental
degradation from  point and   non-point   sources  of
pollution. This  work  provides the new or  improved
technology required  for the control and treatment
of pollution  sources  to  meet environmental guality
standards.

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                                                    EPA 670/2-73-082
                                                    February 1974
           NEW MICROBIAL INDICATORS OF WASTEWATER
                  CHLORINATION EFFICIENCY
                              by

                   Richard  S.  Engelbrecht
                      David H. Foster
                     Elaine 0. Greening
                          Sal H. Lee
                   University of Illinois
                   Urbana,  Illinois 61801
                     Project  17060  EYZ
                   Program Element  1BB043
                      Project Officer

                       C. W. Chambers
           U. S.^Environmental Protection Agency
          National  Environmental Research Center
                  Cincinnati, Ohio 45268
                        Prepared for

            OFFICE OF RESEARCH AND DEVELOPMENT
          U. S. ENVIRONMENTAL PROTECTION AGENCY
                  WASHINGTON, D.C. 20460

For sale by the Superintendent of Document!, U.S. Government Prmtmi Office. Waihtafton, D.C. 30WJ - Price »1.15

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                          EPA Review Notice
This report has been reviewed by the Environmental Protection Agency
and approved for publication.  Approval does not signify that the
contents necessarily reflect the views and policies of the Environ-
mental Protection Agency, nor does mention of trade names or commer-
cial products constitute endorsement or recommendation for use.
                                   11

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                               ABSTRACT
The conform group of indicator organisms has  a relatively  low  resistance
to chlorine when compared to pathogens such as enteric  viruses  and  proto-
zoan cysts.  Consequently, an effort has been  initiated to  find a new
chlorine resistant bioindicator of wastewater  chlorination  efficiency.
Organisms surviving chlorination of wastewater effluents to a free  chlor-
ine residual were collected for study by plating on  various growth  media.
This procedure provided 135 chlorine resistant isolates for further
examination.  A yeast and two different acid-fast bacilli were  found to
be resistant to chlorination in the range considered necessary  for  the
inactivation of pathogens, including viruses.   One acid-fast bacillus
survived 2.0 mg/£ free chlorine for 67 min while the other  survived 1.0
mg/t free chlorine for 15 min.  The yeast resisted 1.0  mg/£ free chlorine
for 20 min.  In comparison, a pure culture of  E. coLi failed to survive
5 min contact with 0.03 mg/£ free chlorine.  Yeasts  were found  to be easily
cultured on acidified yeast extract-malt extract agar.   Acid-fast staining
of colonies on membrane filters incubated on mineral-propionate medium,
following sample pretreatment with oxalic acid and NaOH provided a  selec-
tive assay technique for acid-fast organisms.   Significant  quantities  of
yeasts and acid-fast organisms were found in wastewater effluents and
yeasts have been isolated from stools.  The chlorine resistance and other
characteristics of the yeasts and acid-fast bacilli  under study suggest
that they show promise as bioindicators for wastewater chlorination
efficiency for the more chlorine resistant pathogens.  This report was
submitted by the University of Illinois at Urbana-Champaign, Department
of Civil Engineering, in fulfillment of Project Number 17060EYZ under the
sponsorship of the Environmental Protection Agency.

This report was submitted in fulfillment of Project Number  17060 EYZ by
the University of Illinois under the sponsorship of the Environmental
Protection Agency.  Work was completed as of July 3, 1973.

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                               CONTENTS
Section                                                           Page
  I       Conclusions                                               1
  II      Recommendations                                           3
  III     Introduction                                              5
               Relative Resistance of Conforms  and Viruses          5
               to Chlorine
               Relative Resistance of Conforms  and Vegetative       6
               Bacterial Pathogens to Chlorine
               Resistance of Cysts to Chlorine                      6
               Resistance of Acid-Fast Bacilli to Chlorine          7
               Prevalence of Yeasts and Acid-Fast Organisms  in       8
               Fecal Material and Wastewater
               Objectives of this Study                             10
  IV      Materials and Methods                                     13
               Measurement of Chlorine Residuals                    13
               Isolation of Chlorine Resistant Organisms            13
               Culturing of Chlorine Resistant Isolates             14
               Screening of Isolates for Chlorine Resistance        14
               Detailed Chlorlnation Studies                        16
               Enumeration of Potential Indicator Organisms          16
               in Human Fecal Material and Wastewater
  V       Results and Discussion                                    23
               Isolates Examined for Chlorine Resistance            23
               Further Examination of Isolates from Chlorinated     23
               Wastewater
               Enumeration of Yeasts 1n Fecal Material and          37
               Wastewater

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                          CONTENTS (continued)
Section                                                            Page
               Selective Techniques for Enumeration of              50
               Acid-Fast Bacilli
  VI      Acknowledgements                                          59
  VII     References                                                6'!
  VIII    Publications and Patents                                  67
                                   VI

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                              FIGURES
                                                                  Page

1   Response of Isolate No.  30 to Free Chlorine Residuals          27
    Ranging from 0.1 to 1.0 mg/Z

2   Response of Isolate No.  30A to Free Chlorine Residuals         28
    Ranging from 0.1 to 1.0 mg/£

3   Response of Isolate No.  82 to Free Chlorine Residuals          29
    Ranging from 0.1 to 1.0 mg/£

4   Response of Isolate No.  132 to Free Chlorine Residuals         30
    Ranging from 0.1 to 1.0 mg/2,

5   Response of Isolate No.  134 to Free Chlorine Residuals         32
    Ranging from 0.5 to 2.0 mg/£

6   Free Chlorine Residuals and Contact Times Necessary for        33
    99.9 Percent Kill for Isolates No.  134, No. 30A, No. 132,
    and No. 30 as well as for Organisms Compiled by Berg

7   Comparison of Response of E. co-tt ATCC-11229 to Free           35
    Chlorine with Data from Butterfield et o£.

8   Chiorination Study of Isolate No. 30 Seeded in Diluted         38
    Secondary Effluent
                                  VII

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                                TABLES
No.                                                                Page
 1   Conditions of Isolation and Properties of                      24
     Representative Isolates
 2   Chlorination Stucfy of Isolate No. 30 Seeded in                 36
     Secondary Effluent
 3   Examination of Fecal Samples for Total Plate Count             39
     and Yeasts
 4   Statistical Analysis of Fecal Yeast Densities                  40
 5   Yeast Densities in Raw Municipal Wastewater                    42
 6   Yeast Densities in Activated Sludge Effluent                   43
 7   Yeast Densities in Trickling Filter Effluent                   44
 8   Total Bacteria and Coliform Content in Raw                     45
     Municipal  Wastewater
 9   Total Bacteria and Coliform Content in Activated               46
     Sludge Effluent
10   Total Bacteria and Coliform Content in Trickling               47
     Filter Effluent
11   Pre-Screening for Chlorine Resistance of Yeasts                49
     Isolated from Unchlorinated Wastewater Samples or Stools
12   Effect of Selective Pretreatment Methods on Growth             52
     of Acid-Fast Isolates
13   Effect of Selective Media on Growth of Acid-Fast               54
     Isolates
14   Effect of Sulfa Drugs in Selective Media on Growth             56
     of Acid-Fast Isolates
                                   viii

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                              SECTION  I

                             CONCLUSIONS


1.   EAcAe/u.c/u.a c.oti is not sufficiently  resistant  to chlorine to be
a useful bioindicator of wastewater chlorination  efficiency  for chlorine
resistant pathogens such as viruses.

2.   Contact of wastewater for 5 min with  sufficient chlorine  to  satisfy
a portion or all of the chlorine demand  is a feasible means  of screening
out chlorine sensitive organisms from  wastewater. Moderately  to  highly
chlorine resistant organisms surviving this procedure may  then be col-
lected for detailed study.

3.   The degree of chlorine resistance of  organisms  collected  in  the
screening procedure is not well  correlated with the  chlorine dosage  used.

4.   The majority of chlorine resistant  organisms collected  as potential
new indicator organisms were gram positive sporeformers;  these were  not
studied further due to the dependence  of the sporeforming  property on
generally uncontrollable biological factors.

5.   A yeast, Isolate No. 30, and two  acid-fast bacilli,  Isolate  Nos.  132
and 134, were found to be sufficiently resistant to  free  chlorine resid-
uals in chlorine demand free water to  be potentially useful  as bioindi-
cators of wastewater chlorination efficiency.

6.   Isolate Nos. 30, 132 and 134 show resistance to free chlorine equal
to or greater than that reported for resistant pathogens  such as  Coxsackie
A2 virus; the isolates are able to withstand 1.0 mg/£ free chlorine  in
chlorine demand free water for up to 15, 15, and 60  min contact  time,
respectively.

7.   Yeast organisms could be selectively  cultured from secondary efflu-
ents on yeast extract-malt extract glucose agar adjusted  to  pH 3.5 and
incubated at 20°C; however, growth of acidophilic molds caused some  inter-
ference in enumeration.

8.   Yeasts were isolated  from human fecal material  in concentrations  up
to 10^ yeasts per g in 80  percent of 31  samples tested.

9.   Yeasts were isolated  from wastewater in average concentrations  of
1500, 220, and 420 yeast per mi of raw wastewater, activated sludge and
trickling filter effluents, respectively.

10.  Use of sample pretreatment by acidification with 2.5 percent oxalic
acid for 5 to 10 min followed by neutralization with 2 percent NaOH con-
siderably reduced the number of contaminating organisms for the enumeration
of acid-fast bacteria in wastewater.

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11.  A method for acid-fast staining of membrane filters was  developed
and, v/hen combined with oxalic acid-NaOH pretreatment  and  selective media,
provided a sensitive and selective method for enumeration  of  acid-fast
bacteria in wastewater.

12.  Limited studies of raw wastewater indicated the presence of  acid-
fast bacteria in concentrations of 137 to 500 per mfc.

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                              SECTION  II

                           RECOMMENDATIONS
1.   Chlorine resistant organisms  isolated thus  far  require further
evaluation as to their resistance  in  a  variety of wastewater  effluent
types.

2.   The membrane filter technique for  enumerating acid-fast  bacilli
should be thoroughly studied as  to its  sensitivity,  reliability and
accuracy in highly contaminated  samples such  as  wastewater.

3.   A method for inhibiting mold  growth in assaying wastewater efflu-
ents for chlorine resistant yeasts is needed.

4.   The quantities of proposed  indicators in fecal  material, and
various types of wastewater effluents,  including AWT type effluents,
in a variety of climatic and geographical  situations, should  be
determined.

5.   Taxonomic studies of the proposed  indicators should be  carried  out.

6.   Proposed indicators should  be evaluated  under field conditions  in
a variety of water quality situations for appropriate sampling methods,
the need for and type of sample  concentration techniques, and proper
sample storage procedure.

7.   Laboratory scale studies of the response of the proposed indicator
organisms to AWT processes is necessary to provide information on their
usefulness in water reuse schemes.

8.   The response of the proposed indicators  to disinfectants other
than chlorine should be studied.

9.   The resistance of the proposed indicator to disinfectants should
be directly  compared to that of resistant pathogens; comparison of the
relative survival rates of the indicators and pathogens in receiving
water  is needed.

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                             SECTION III

                             INTRODUCTION
The presence of pathogenic organisms in the effluents  of conventional
secondary and advanced wastewater treatment operations which  may  be
resistant to the widely used chlorine disinfection process  is a matter
of increased concern.  It is presently anticipated that direct reuse
of reclaimed wastewater effluents for potable water supplies  will  be
necessary in the foreseeable future in many areas of this country due
to rising population and increased per capita water demand.   A reliable
biological indicator of the efficiency of the wastewater disinfection
step is one approach that can be used to protect the health  of popula-
tions using reclaimed wastewater for potable water supplies  and  also  to
alleviate public health fears of people using waters receiving chlorinated
waste effluents for other purposes such as contact recreation.


RELATIVE RESISTANCE OF COLIFORMS AND VIRUSES TO CHLORINE

The literature indicates that the presently used coliform group  of
organisms is far too sensitive to chlorine to be of much value in
indicating the potential presence of chlorine resistant infective
agents such as viruses.  At low temperatures, i.e. 0° to 6°C, polio  1
and Coxsackie A2 viruses are much more resistant to chlorine than
EAch&U.chj,a, cati while adenovirus 3 is apparently more sensitive (1,  2).
Nupen (3) concluded that coliform findings should not serve as a measure
of the virus contamination  in water and sewage.  Liu vt at. (4)  studied
the chlorine resistance of  20 human enteric viruses seeded in Potomac
River water.  The least chlorine resistant virus, reovirus I, required
only 2.7 min contact with 0.5 mg/Jl free chlorine for a 99.99 percent
kill, assuming first order  kinetics.  The most chlorine resistant viruses
were poliovirus 2 and  Coxsackie B5 which required 40 min to reach the
same kill as the reovirus under the same conditions and assumptions.
Experimentally, Coxsackie A5 and echovirus 12 survived these conditions
for 53.5 and more than 60 min, respectively.  Kruse'  (5) compared the
chlorine resistance of bacterial virus f2 and E. coti under a variety
of experimental conditions.  E. co&t was found to be considerably more
sensitive to inorganic and  organic chloramines at 0° to 4°C than the
model virus.  For example,  the density of E. coJU decreased nearly 5
logs in less than 1 min while the model virus f2 was  inactivated to
slightly more than 1 log following  10 min contact with 10 mg/£ chlorine
in the presence of 10~3 M NHaCl.  The work of Kruse'  demonstrated that
inactivation rates are considerably reduced  for  both  E.  (Loti  and virus
when the combined chlorine  residual is organic   chloramine as opposed
to inorganic forms.  Kjellander and Lund  (6) have reported similar
findings for E. cjoti and poliovirus 3.  Burns and Sproul (7)  found that
bacteriophage T2 was considerably more resistant  to free chlorine than

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 E,  c.oti.  The  resistance  of viruses  to chlorine appears  to vary widely.
 Thus,  if  a  full  assessment  of the relative  value of an  indicator organism
 is  to  be  made, the  chlorine resistance of all  enteric viruses  must be
 studied.  The  data  that do  exist  suggest  that,  with few exceptions,
 viruses are more resistant  to chlorine than coliforms by a considerable
 margin.


 RELATIVE  RESISTANCE OF COLIFORMS  AND VEGETATIVE  BACTERIAL  PATHOGENS TO
 CHLORINE

 The resistance of wastewater pathogens other than virus  to chlorine is
 quite  variable.   Kabler (8)  compared the  chlorine resistance of E.  c.oti,
 keAjobacteA a&Loge,neA, ?&o.u.domoYia&  a&iu.&ino&a, SatmoneJtJta typho&a,  and
 SklQoJUUi  dyAe.ntVu.ae. and Aonn&L.   At pH 7 and  20° to 25°C,  resistance
 to  free chlorine was approximately the same for E.  coti  and ?.  aeAu.g4.noAa
 but was less than that found for  S. typho&a and Sh^igelta dyAe.nteJu.ae..
 Resistance to  combined chlorine was  comparable  for E. a>tL,  P.  a&suiQ4.noAat
 Skig<a AonneA.,  and S. typkoAa,  while Skigetta dyAe.nteAA.ae. was more
 sensitive than the  others.   A. aeAogeneA  was more resistant to both  com-
 bined  chlorine and  free chlorine  than  the other bacteria studied.   Tonney
  were 5  to 20  times more
 resistant to chlorine than  coliforms.   Favero  and his associates (11.  12)
 showed Staph. awieuA to be more resistant to chlorine than  either coli-
 forms  or P. aeAag
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           . and species of the HoA^ane££a-Waeg£eAta group  are  pathogenic
protozoans of man capable of being transmitted by the water route  (16).
Chang (17) reported that cysts were 160 times more resistant to HOC1
than E.  coti and 9 times more resistant than the hardier entero viruses.
Hypochlorous acid residuals at 1.2 mg/£ for 30 min contact  were required
to kill  100 percent of E. ki&tofytica. cysts  at 23° C in one study  (18).
Stringer (16)  compared the cysticidal properties of 2 mg/JZ, each of free,
combined inorganic and combined organic chlorine at pH 7 and 27°C  and
observed that a 10 min and 40 min contact time was necessary for a 99
percent kill for the first two categories, while organic chloramines
failed to destroy more than 50 percent of the cysts even after  100 min
contact.  Cysticidal activity was greatest at low pH.  Although the high
degree of resistance which amoebic cysts have to chlorine should be a
matter of concern, it should be noted that they are generally effectively
removed by coagulation-sedimentation and filtration (19).  In addition,
they occur in cyst contaminated waters at levels not likely to  be  greater
than 5 cyst per ma (20).  Since the cysticidal chlorine dose greatly
depends on the quantity of cysts present, and, since most investigations
have employed cyst concentrations  greatly in excess of those that might
be expected to occur naturally, it is likely that reported  cysticidal
doses are greater than those required in the field.


RESISTANCE OF ACID-FAST BACILLI TO CHLORINE
              spp. and NocaAdia. spp. are acid-fast organisms which have
been recovered from fecal material and wastewater (21, 22).  Hycabac.-
teAiw tubvicu£oA4A is of major concern from a public health standpoint
while other members of the acid-fast genera may be pathogenic depending
on various biological factors.  Mycobacteria differ from other vegeta-
tive bacteria in that they have protective layers of mycolic acid and
lipids in their cell walls (23).  These cell wall constituents confer
a degree of resistance of mycobacteria to chemical agents such as chlor-
ine that are generally not found in other vegetative bacterial groups.
Musehold (24) found 17 mg/£ was insufficient while 340 mg/£ was suffi-
cient to kill tubercle bacilli following a 2 hr contact in sewage
samples.  Kabler  (25) found that up to 2 hr contact with 1 to 2 mg/£
chlorine was necessary to achieve a 99 percent inactivation of M. -tubeA-
cjuJto&iA.  Greenberg and Kupka (26) reviewed about 15 different studies
which led them to conclude that a chlorine dosage of 20 mg/Jl with a 2
to 3 hr contact time or a chlorine residual of at least 1 mg/JJ, after
1 hr contact were the conditions necessary to destroy all tuberculosis
organisms.  If these organisms are of concern from a public health
standpoint, then  higher chlorine residuals and longer contact periods
are required to inactivate tuberculosis organisms in comparison to those
needed to destroy enteric bacteria.

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 PREVALENCE  OF YEASTS  AND ACID-FAST  ORGANISMS  IN  FECAL  MATERIAL AND WASTEWATER

 Two groups  of organisms  which  this  study  has  shown  to  have  potential as
 chlorine  resistant  bioindicators  are yeasts and  acid-fast bacilli.
 Studies of  their occurrence  in  fecal material  and wastewater are  rather
 limited,  and  knowledge of acid-fast organisms  in these materials  has
 focused principally on the tubercle bacilli.

 Cooke  (27)  reviewed the  occurrence  of yeasts  in  a variety of habitats
 and reported  that they occur commonly in  the  alimentary tracts of higher
 animals which ingest  them with  their food.  Saprophytlc yeasts are able
 to  pass through the digestive tract relatively unscathed by the acid
 conditions  in the stomach.   Asporoo/enous  type yeasts  appear to pre-
 dominate  in human feces.   While fecal yeasts  are generally retained no
 longer than ingested  food, pathogenic strains  of Candida. atbwJtop&t Candida,  and TxAchoApoJton frequently
encountered.
                                   8

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Add-fast organisms are of interest because of their reported  chlorine
resistance and the possible pathogenicity of some .Voco/tdca and Ito/cobac-
tutAW species.  Reports of tubercle bacilli in feces date back to  at
least 1900.  Reports of add-fast bacilli in feces other than  the
tubercle bacilli are quite sparse.  Klose (33) found acid-fast bacilli
in the stools of 55 of 60 patients showing sputum positive for tubercle
bacilli.  No acid-fast bacilli  were found in 12 fecal specimens from
persons with sputum negative for tubercle bacilli.  Alexander  (34)
found acid-fast organisms 1n stools of 38 of  45  pulmonary tubercu-
losis patients.  Laird vt ad.  (35) reviewed similar studies and reported
that the majority of patients showing positive sputum specimens also
provided stool specimens which contained add-fast organisms.   Acid-fast
organisms were not frequently found 1n the feces of healthy persons.
Wilson and Rosenberger (36) detected acid-fast organisms 1n 21 percent
of over 1000 fecal samples from apparently healthy individuals.  Laird
it aJL. (34), on the other hand, found acid-fast organisms in the feces
of only 2 of 54 persons with negative sputum.  It should be noted that
these findings are quite outdated in terms of techniques employed.   It
1s quite possible that the use of more modern methods not specifically
aimed at finding tubercle bacilli but more generally towards isolating
all potential acid-fast organisms would show a greater percentage of
the healthy population to be excreters of acid-fast organisms,

Several investigations on the presence of tubercle bacilli 1n wastewater
have appeared 1n the literature.  Musehold (24) added tubercle bacilli
to river water, sewage, and sewage sludge and exposed the samples to
prevailing environmental conditions.  Viable bacilli were recovered from
river water and sewage sludge even after 5 months and 6 1/2 months
exposure to these conditions, respectively.  Bacilli were also demon-
strated 1n the effluent from a secondary wastewater treatment plant.
Jensen and Jensen (21) were consistently able to recover viable M.
tubvicutjo&ii> 1n effluents from sanatoria following biological  treatment,
even when the populations of aerobic enteric bacteria had been reduced
to 0.2 percent of their original numbers.  These authors also determined
that 10 of 10 samples each from raw sewage and activated sludge effluent
from a sanitorlum treatment plant were positive for tubercle bacilli
while only 1 of 10 samples from the chlorinated effluent contained
detectable quantities of these organisms.  Dosage was 10 mg/i chlorine
with a contact in excess of 3 hr.  Pramer vt aJL. (22) reported that
avian tubercle bacilli seeded into raw wastewater was not removed by
6 hr of settling.  Chemical coagulation with ferric  chloride at pH 5.0
resulted 1n removal of 99 percent of the bacilli as did sand filtration.
On the other hand, aeration of the wastewater for 24 hr in laboratory
biological treatment units had little effect on the  density of tubercle
bacilli.  Free chlorine residual disinfection of the wastewater was neces-
sary to achieve significant reduction of the bacilli.  The authors noted
that free residuals and dosages used were considerably higher than that
normally maintained for disinfection of ordinary municipal wastewater.

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 The authors  studied  a tuberculosis  sanitorium trickling filter plant and
 found 1500 M.  tub&iculoA  organisms  per mi  in the raw waste which were
 reduced to 10  per mi in  the chlorinated plant effluent.  However, the
 raw sludge had 100,000 organisms  per  m£ indicating that while removal
 may have appeared to be  efficient,  tremendous quantities of viable path-
 ogens had been concentrated in  the  sludge.   Digestion of the sludge was
 only able to reduce  the  M.  tubeAculoAit* density to 10,000 per mfc.  Mu'ller
 (37) reported  that raw wastewater contained  5 to 100 tubercle bacteria
 per liter compared to 100 times as  many SaAnonztla. organisms in the same
 volume.  She stated  that tubercle bacteria must be considered to be a
 regular component of urban  wastewater, even  without known sanitaria
 sources.  The  investigator  found  90 percent  of the raw wastewater and
 50 percent of the settled wastewater  samples to be positive for tubercle
 bacilli.  On the other hand,  sludges  subjected to 30°C under septic con-
 ditions showed no tubercle  bacilli.   Sludge  samples taken from drying
 beds used for  waste  activated sludge  were 44 percent positive even after
 30 days drying time.   It would  appear from these studies that while
 biological treatment may be counted on for some removal of acid-fast
 organisms, both the  effluent  and  the  resulting sludges will contain
 viable organisms.  Chlorination of  the effluent with high dosage at
 extended contact periods may  provide  a safe  effluent.


 OBJECTIVES OF THIS STUDY

 The  major  objective of Chlorination of wastewater effluents is  to pro-
 duce an effluent that is acceptable from a public health standpoint.
 In order to  assess the efficiency of wastewater Chlorination in terms
 of destruction  of pathogens, there is  a need for a reliable bioindicator
 which  is at  least as resistant to chlorine as the most chlorine resis-
 tant  pathogens.  The bioindicator should also be rapidly and unambigu-
 ously  quantifiable in chlorinated effluents  by simple and easily applied
 techniques.  Since it would appear that coliforms,  the most commonly
 applied  group of bioindicators,  do not meet  the criterion of being as
 resistant to chlorine as the most resistant  pathogens,  the suitability
 of coliforms  for judging the efficiency of wastewater Chlorination may
 be seriously questioned.   This is particularly true where wastewater
 reuse  schemes are being considered,  since,  in these situations,  protec-
 tion of  the public health is paramount.

The coliform organisms have been quite helpful  in  the past in providing
 information on the potential presence  of bacterial  pathogens  in  many
 types of waters.  However,  it would  seem appropriate  in  light of their
 inability to  satisfy the public  health needs  in many  situations  to re-
evaluate their application  on a  case-by-case  basis.   It  is  suggested,
therefore, that the indicator organisms  should be selected for  use on
the basis of the purpose  and information required,  e.g.,  the  inactiva-
 tion of resistant pathogens  by Chlorination.   It was with  this  purpose
 in mind that  this study was  undertaken.
                                   10

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It need not be emphasized that the majority of results  obtained  in  this
study are of a negative nature.   This  is  to be expected in  a  search  study
of this type.  It may be pointed out that several  decades were required
to develop the coliform test to its present state of refinement, with
many false leads and pitfalls along the way.  The negative  results  pre-
sented here may help other investigators  to avoid the expenditure of
research efforts in areas that show little promise of a successful  outcome.
On the other hand, it is felt that several  promising developments towards
the realization of a new indicator of wastewater chlorination efficiency
have arisen from this study.  The original  objective of the study to find
an organism(s) that is as resistant to chlorine as the most resistant
pathogens and to develop rapid,  simple, sensitive and selective  procedures
for their enumeration in secondary and advanced waste treatment  effluents
has been met at least in part.  Further study will be required  to refine
techniques and to test the validity of the proposed wastewater  indicators
under a variety of field conditions.  The techniques developed  in this
study have provided several candidate indicator organisms  for measurement
of chlorination efficiency and,  thus,  have considerably expanded the
available alternatives in assessing the public health quality of chlori-
nated effluents.
                                   11

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                              SECTION  IV

                      MATERIALS AND METHODS
MEASUREMENT OF CHLORINE RESIDUALS

The measurement of chlorine residuals in secondary effluents  was  found
to be most satisfactory when the DPD (N,N-dimethyl-p-phenylene-diamine
monohydrochloride obtained from Eastman Kodak Company,  Rochester,  New
York) colorimetric method (38,39,40,41) was used because both free and
total chlorine residuals can be determined in the same  samples within a
2 min period.  It should be noted that high levels of chloramines  may
interfere with this procedure, yielding a higher apparent free chlorine
residual than is actually present.  Oxidation-reduction potential  measure-
ments were employed to confirm the reliability of this  method.

It is generally accepted that the amperometric method of measuring chlo-
rine residuals is the preferred procedure in studying the response of
microorganisms to chlorine when precise information is  desired (7,39,42).
Burns and Sproul (7) conducted a study in which chlorine residuals
determined by amperometric titration showed a constant relationship to
organism destruction whereas orthotolidine-arsenite  (OTA) residuals
did not.  Chambers (43) found that if the amperemeter was "sensitized"
before use by repeated chlorine residual measurements, i.e. 15 times,
using a solution having approximately the same concentration of chlorine
as the test solution, chlorine concentrations as low as 0.005 mg/Jl could
be detected.  An amperometric titrater (Wallace and Tiernan, Inc.,
Belleville, New Jersey) was used to measure chlorine residuals in the
controlled chlorination studies carried out with chlorine demand free
water.  The procedure for amperometric titrations described in Standard
M&tkod& (44) was followed.
 ISOLATION OF CHLORINE RESISTANT ORGANISMS

 Several activated sludge and trickling filter effluent samples from the
 East Side Treatment Plant of the Urbana and Champaign Sanitary District
 and a sample of oxidation pond effluent from the Decatur Sanitary District
 Sewage Treatment Plant were the main sources of potential indicator
 organisms.  These samples were filtered through several layers of cheese-
 cloth and stored at 10°C for never more than 5 hr before chlorination.
 The different effluent samples were chlorinated either to satisfy part
 of the demand by adding from 6 to 63 mg/Jl of chlorine or to reach a free
 chlorine residual of 0.15 to 8.0 mg/Jl by adding from 75 to 176 mg/£ of
 chlorine as sodium hypochlorite for contact periods of 5 to 30 min at
 either room temperature or 20.5°C.  Following dechlorination with an
 excess of 0.05N_ sodium thiosulfate, aliquots were plated on several types
 of media.  These included nutrient agar and tryptone-glucose agar
                                    13

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 from Difco  Laboratories  (Detroit,  Michigan) and trypticase-soy agar, WL
 Differential  agar,  and Middlebrook and  Cohn 7H10 agar from BBL (Cockneys-
 vilie,  Maryland).   Media prepared  in  the laboratory included starch agar
 (0.5 percent  peptone, 0.5 percent  yeast extract, 0.3 percent soluble
 starch,  1.5  percent agar),  nitrate agar (1 percent peptone, 0.5 percent
 yeast extract,  0.4  percent potassium  nitrate, 1.5 percent agar), and
 succinate agar  (0.2 percent  NH^N03, 0.1 percent KgHPO*, 0.02 percent
 MgS04,  0.5  percent  sodium succinate,  1.5 percent agar;.  The agar was
 obtained from Difco Laboratories and  the other chemicals from Mallinckrodt
 Chemical Works  (St. Louis,  Missouri).   Double strength nutrient agar
 adjusted separately to pH 3, 5, 7,  and  9 was also used.  The streaked
 plates were incubated at 10°,  20°,  37°, and 45°C for 24 to 96 hr.


 CULTURING OF  CHLORINE RESISTANT ISOLATES

 Organisms that  grew on the originally inoculated plates, following chlor-
 ination  of  the  effluent,  were  examined by a phase-contrast microscope for
 morphological characteristics, Gram stained, and subcultured to obtain
 pure cultures.  Stock cultures were made on nutrient agar slants and
 stored at 5°C.  Subcultures  collected for detailed study were periodically
 transferred to  fresh agar slants.

 In preparation  for  controlled  chlorinatlon experiments, the extinction
 coefficient of  each isolate was determined.  This was accomplished by
 growing  each  organism in  nutrient  broth on a shaker and, after an appro-
 priate incubation period, the  culture was centrifuged and the cells
 washed twice  and resuspended in phosphate buffered water at pH 7.  The
 optical  density of  the suspension was measured at 660 n.m.  in a Spectronic
 20 spectrophotometer and  various dilutions were plated in nutrient agar
 pour plates.  The data obtained from pour plate colony enumeration were
 correlated  with the optical density to obtain the extinction coefficient.


 SCREENING OF  ISOLATES FOR CHLORINE  RESISTANCE

 Pure cultures of isolates were examined as to their specific resistance
 to chlorine.  Several types of water were considered for use as the basic
 suspending  menstrum, including 1)  raw ground water aerated to precipitate
 ferric iron, membrane filtered, and buffered to pH 7; 2) water prepared
 in the same manner as No. 1 but autoclaved after pH adjustment; 3)  auto-
 claved distilled water buffered to pH 7; and 4)  physiological saline pre-
 pared from  deionlzed water buffered to pH 7.  However,  for various  reasons
 these waters were found to be unsatisfactory.   On the other hand, it was
 found that  the requirements  for these studies could be met best by using
 the  chlorine demand free water as  developed by Butterfield e£ at.  (45),
 the  complete preparation  of which  was described by Megregian (46).

The  glassware was washed with Haemosol (Melnecke and Company, New York)
                                   14

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and then soaked in a strong chlorine solution (75-150 mg/fc)  for  at
least 2 hr before rinsing at least 10 times  with  deionized water and
finally with chlorine demand free water (43).   Glassware used with
chemicals, potentially toxic to the organisms under investigation,
was soaked overnight in cleaning acid (35 m£ of saturated sodium di-
chromate in 1 a of concentrated sulfuric acid)  and then  rinsed with
water.  Sterilization was accomplished in a  dry hot air  oven at  190°C
for 2 hr.

Prior to a chlorination experiment, the isolate to be  examined was
grown overnight in an aerated nutrient broth culture.  The washed sus-
pension was then diluted on the basis of cell concentration  as deter-
mined by optical density measurements and 1  m£ aliquots  were added  to
the test flasks so as to have a final cell concentration of  103  to
104/m£ in the flasks.

The response of the various isolates to chlorine  was determined  using
essentially the same procedure described by  Butterfield  &t oJL.  (45).
A determined amount of chlorine and a test organism were added  to a
number of sterile 1 £ erlenmeyer flasks, each containing 500 to  700 m£
of sterile chlorine demand free water.  Two  control flasks were  treated
in the same manner except that one received  only  chlorine  and the other
only the test organisms.  The flasks were incubated in a water  bath at
20.5°C.  The preliminary screening was originally performed  using
chlorine dosages of 0.1, 0.5, and 1.0 mg/&,  but was later changed  to a
single dosage of 0.5 mg/fc so that three or more isolates could  be
screened at one time.  Later to facilitate the screening of  isolates,
chlorination experiments were done with a mixture of morphologically
similar organisms in one reaction flask.  Those isolates showing some
resistance at 0.5 mg/Jl free chlorine residual were then further screened
as to chlorine resistance with the three chlorine concentrations men-
tioned above.  The free chlorine residuals were measured by  amperometric
titration after 5 and 30 min contact.  In this phase of study,  1 ma
aliquots were removed from the test flasks at 5,  15, and 30  min  intervals,
dechlorinated with excess 0.025 N thiosulfate in  a fivefold   dilution,
diluted  tenfold further in pH 7 phosphate buffer, and plated on agar
pour plates using an appropriate nutrient medium.  Replicate plates of
each dilution were made and incubated for 24 to 48 hr.  Promising  iso-
lates were subjected to more detailed studies with chlorine dosages  of
0.1, 0.3, 0.5, 0.7, and 1.0 mg/Jl with removal of 1 mfc aliquots  at  5, 10,
15, 20, and 30 min intervals.  Further studies employed higher chlorine
concentrations and longer exposure times depending on the chlorine resis-
tance of the particular isolate.  The entire selection procedure from
the chlorination of effluent to the final chlorination experiments  using
high chlorine dosages in chlorine demand free water, provided a means of
continually eliminating organisms which were unsuitable due to  low chlo-
rine resistance and other undesirable properties.
                                   15

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 DETAILED CHLORINATION  STUDIES

 Using the most promising  organisms,  six  separate sets of experiments were
 carried out  to obtain  further  information  concerning their properties,
 The purpose  of one group  of  experiments  was to  determine the length of
 time and concentration required  for  99.9 percent kill of the test organism.
 The contact  times  were increased to  as much as  200 min and the chlorine
 concentrations up  to 2 mg/£.

 A culture of E.  wti ATCC-11229,  obtained  from  the National Environmental
 Research Center  in Cincinnati, Ohio, was examined for its resistance using
 concentrations of  free residual  chlorine of 0.01 to 0.04 mg/Jl at a cell
 concentration  of Kr/mJl.  Samples were taken following 1, 5, 10, 15, 20,
 and 30 min of  exposure to chlorine.  This  organism was employed due to
 its previous use by other investigators  so as to allow comparison of results.

 Mixed culture  chlorination experiments were carried out using yeast isolate
 No.  30 and E.  c.oti ATCC-11229 to  study survival at chlorine concentrations
 of 0.02,  0.1,  and  0.5  mg/A.  These two organisms were added together in
 the same reaction  flasks; the concentration of  E. coti was 5000/mA and
 that of No.  30 was 1000/mJi.  Organism survival  was determined after 1, 5,
 10,  15,  20,  and  30 min  contact with the  chlorine.  To distinguish between
 the two organisms, samples were  plated on  EMB agar on which only E. cjoti
 gives  the lactose  reaction and on nutrient agar adjusted to pH 3.5 with
 d-tartaric acid  (J. T.  Baker Chemical Company,  New Jersey) for detection
 of Isolate No. 30.

 The appropriateness of  a potential new indicator organism as applied to
 wastewater chlorination was evaluated through studies of its Chlorine
 resistance when  seeded  in secondary effluent.   In experiments involving
 the  use  of yeast Isolate No. 30, chlorine  residual  measurements were made
 using  the  DPD  method.  The apparent free chlorine residuals measured in
 these  experiments may  have been due, in  part, to interference caused by
 high  concentrations of  chloramines.   However,  the alternative ampero-
metric method  was  found to produce unreliable results due to an indis-
tinct  endpolnt when used for chlorine measurements with the wastewater
samples.   In order to reduce the chlorine demand and the production of
chloramines, wastewater effluents were diluted tenfold prior to chlorina-
tion.  This  dilution probably provided a quality water that might be
similar to an AWT type effluent.  Chlorine dosage could thus be markedly
reduced while  still allowing the attainment of free chlorine residuals.
Thus, meaningful  survival  curves for resistance to free chlorine could be
obtained.
ENUMERATION OF POTENTIAL INDICATOR ORGANISMS IN HUMAN FECAL MATERIAL
AND WASTEWATER

For a test organism to be a suitable indicator of fecal  contamination,  it
                                   16

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should be routinely present in human fecal  material  and  also  in domestic
wastewater.  Therefore, both stool  samples  and  wastewater were examined
for the presence of yeasts and acid-fast  bacteria, two groups of isolates
which showed chlorine resistance at levels  considered necessary for  inac-
tivation of pathogens,  including viruses.


Yeast Enumeration in Fecal Material and Wastewater

Because the growth of the majority  of bacteria  and actinomycetes is
inhibited at pH values  less than 4.5 while  yeasts and molds are not, a
selective enrichment medium yeast extract-malt  extract glucose agar  (YMA)
(yeast extract 0.3 percent, malt extract  0.3 percent, glucose 1 percent,
peptone 0.5 percent, agar 2 percent) which  had  been  adjusted  to pH 3.5-
4.0 with 1 N HC1 was used as the medium of  choice for yeast enumeration
in both fecal samples and wastewater.  Initially the acid medium used
was potato dextrose agar adjusted to pH 3.5 with 10  percent tartaric
acid.  Wickerham (47) recommended that yeast extract-malt extract  glucose
agar (YMA) be used as the medium of choice  for  yeast enrichment when the
pH is lowered to the acid range (pH 3.5-4.0).   This  medium was evaluated
using yeast Isolate Nos. 30 and 30A.  After daily examination for  the
growth of yeasts in  three acid media, i.e. nutrient agar,  potato-dextrose
agar, and YMA, all adjusted to pH 3.5, it was concluded  that  the rate  of
yeast growth in YMA was the most favorable.

Stool samples were obtained primarily from  two  sources.  Stools  from
individuals, not using any form of therapeutic  drugs but confined  to a
nursing home for reasons other than infectious  medical  problems, were
used.  In addition, stools from healthy university  student  volunteers
were obtained for study.  One to four "wet" grams  of human  feces were
suspended in sterile phosphate buffered water (pH  7) to  yield a  1  to 10
percent suspension and macerated with glass beads  on a  reciprocal  shaker
until  the samples were homogeneously suspended. Serial tenfold   dilu-
tions were made aseptically.  Again, pour plates using YMA-acid media
and diluted stool samples were made; the yeast  colonies  present  after
3 to 5 days incubation at room temperature and 37°C were  counted.

Various samples of wastewater were obtained at  the  East  Side  Treatment
Plant operated by the  Urbana and Champaign  Sanitary District. The major-
ity of wastewater samples, obtained at the plant, were  initially  filtered
through several layers of cheesecloth at the time  of sampling in  the
field and stored at 5°C for not more than 5 hr before  being examined.
In addition, in order  to determine the effect of sample preparation  on
the apparent densities of organisms present in wastewater,  alternate
sample treatment methods were compared to cheesecloth  filtration.
Samples were taken without filtration directly to the laboratory and a
portion of each sample was filtered through several  layers  of cheese-
cloth and vigorously shaken.  The  remaining portion of the sample was
divided into two parts, one of which was homogenized by blending for
about 30 sec while the other was vigorously shaken approximately 25
                                   17

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 times  as  recommended in StundaAd M&tkodt* (44) in order to break the
 bacterial  clumps.  The yeast densities for each sample preparation
 method were then determined and compared.

 Enumeration of yeasts in wastewater was accomplished by the pour plate
 technique  using replicate plates of YMA-acid media and diluted wastewater.
 The yeast  colonies present after 3 to 14 days incubation at 20°C and 37°C
 were determined.
 Development of Selective Techniques for Yeast Enumeration in Fecal
 Material and Wastewater

 Since YMA-acid medium also permits mold growth, difficulty was experienced
 in counting discrete yeast colonies.  Several means of eliminating inter-
 fering contaminants were investigated.

 A mold inhibitor, sodium propionate, was added at a concentration of
 0.25 percent to suppress mold growth.  Sodium propionate was found to
 be not entirely satisfactory in this regard.  An anaerobic incubation
 method with a parafin layer on YMA-acid medium was also evaluated.  To
 eliminate occasional acidophilic bacterial growth on YMA-acid plates,
 an antibiotic, oxytetracycline (Terramycin, Chas. Pfizer Co.) was incor-
 porated into the medium.  Ten m£ of a  0.1 percent solution, freshly
 prepared and sterilized by membrane filtration, was added to 100 m£ of
 melted 45°C YMA-acid medium at pH 3.5.

 In order to compare the relative presence of indicator organisms with
 "normal" wastewater and fecal organisms, a total plate count was made
 in addition to yeast enumeration by preparing duplicate nutrient agar
 pour plates at each of several dilutions and counting the colonies present
 after a minimum 2 days incubation at 37°C.


 Enumeration of Acid-Fast Bacilli in Fecal Material and Wastewater

 Samples of wastewater and stools for the determination of acid-fast
 bacilli densities were obtained and treated essentially the same as for
yeasts as outlined above.


 Development of Selective Techniques for Enumeration of Acid-Fast Bacilli
 in Fecal  Material and Wastewater

A similar problem of contaminants as in the yeast studies was encountered
when stools and wastewaters were examined for acid-fast bacteria.  Three
 approaches were taken to develop selective techniques for enumeration of
acid-fast bacilli.  First,  several  methods of pretreating samples prior
to culturing were examined  as to their relative efficacy in removing
                                   18

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contaminants.  A second approach was to use various  selective  media  for
acid-fast bacilli.  To some of the selective media various  chemical  agents
were added in order to suppress growth of contaminats.   Lastly,  a  tech-
nique was developed for the acid-fast staining of membrane  filters for
positive identification and enumeration of acid-fast organisms.  The
selective methods were evaluated for known acid-fast bacilli obtained
from wastewater prior to study of fecal and wastewater samples.


Methods for the Pretreatment of Samples

Since sputum samples have been routinely examined for the presence of
acid-fast tubercle bacilli for many years, the selective technique
applied to sputum was investigated.  The alkaline sputum treatment
method (48) using 1, 2, 6, and 10 percent NaOH treatment was examined
with known cultures of acid-fast bacilli obtained from secondary efflu-
ents.  Samples were contacted with alkali  for various time periods
and then neutralized with dilute HC1.

In addition, pretreatment of sample with quaternary ammonium compounds
was evaluated to determine the ability of this pretreatment to suppress
growth of contaminants and to assess the ability of acid-fast  organisms
to survive this treatment.  Four quaternary ammonium compounds (QAC),
Arquad T-2C-50, Armeen C, Armeen 12D, and Roccal, were first dissolved
in phosphate buffer and a predetermined amount added to cell  suspensions
for exposure periods of either 5 or 10 min.  These suspensions were
centrifuged to remove the cells from the QAC; the cells were then resus-
pended in buffer and plated in Middlebrook and Cohn 7H10 agar.  Armeen
C and Armeen 12D dissolved more completely in 40 percent ethanol than
in buffer; thus, further experiments with these QAC were carried out
using 40 percent ethanol solutions.

Pretreatment of cultures containing both acid-fast bacteria as well  as
potentially interfering microorganisms with 5 percent oxalic acid for
30 min followed by neutralization with 4 percent NaOH was recommended
by David (49).  Evaluation of this pretreatment was undertaken first
by treating Isolate  Nos. 132 and 134 with oxalic acid-NaOH to determine
their sensitivity.  In order to evaluate oxalic acid-NaOH pretreatment
for wastewater and fecal samples, contact time and the oxalic acid con-
centration were varied.
Development of Selective Media for Enumeration of Acid-Fast Bacilli

Middlebrook and Cohn 7H10 agar is generally considered to be a selective
medium for acid-fast organisms.  However, in highly contaminated speci-
mens, such as wastewater and feces, the selectivity of this medium was
not sufficient to overcome the growth of other, non-acid-fast organisms.
Moreover, the use of oxalic acid-NaOH and the other pretreatment methods
                                   19

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was  found  not to be sufficient because a  number of spore forming
organisms  were observed to survive treatment in wastewater and fecal
samples.   A satisfactory selective medium for acid-fast bacteria is
necessary  due to their low concentration in wastewater in comparison
to contaminant organisms.

Incorporation of chemotherapeutic agents and various dyes into an
enriched acid-fast bacteria medium was investigated.  Two acid-fast
bacilli, Isolate  Nos. 132 and 134, and samples of secondary effluent
were studied separately in Middlebrook and Cohn 7H10 agar containing
penicillin at concentrations from 10 to 250 units per mfc of medium as
well as malachite green and Eosin Y at concentrations of 0.005 to 0.0075
percent.   In addition, several other drugs were tested against the two
acid-fast  bacteria using sensitivity discs impregnated with various
quantities of the drugs.  Impregnated sensitivity discs were placed on
pour plates and the presence or absence of a zone of inhibition was
noted.  Studies of the relative sensitivity of wastewater organisms
and the two acid-fast bacilli to eight antibiotics (chloromycetin,
neomycin,  erythromycin, kanamycin, novobiocin,  penicillin, streptomycin,
and tetracycline with 2, 5, 10, or 30 meg per disc) and eight sulfa
drugs  (sulfamethacypyridazine, elkosin, gantrisin, sulfadiazine, sulfa-
merazine,  sulfa thiazole, thiosulfil and triple sulfa with 50 or 300
meg per disc) were carried out to determine the usefulness of their
incorporation into selective media using the sensitivity disc method.
Additionally, five sulfa drugs (kynex, gantrisin, elkosin, sulfathiazole
and sulfamethizole) were suspended in phosphate buffer, then later in
40 percent ethanol, and a predetermined amount  was incorporated into
Middlebrook and Cohn 7H10 agar.  The resistance of the two acid-fast
bacilli and activated sludge effluent organisms was examined separately
and quantified in terms of survival at various  drug concentrations as
compared to control plates containing no antibiotics or sulfa drugs.

Since many selective culturing techniques are based on information gen-
erated from knowledge of the microbial metabolic pathways, a selective
culturing medium for acid-fast bacilli using organic acids and other
metabolites as the sole carbon source was investigated.  Mineral salt
medium (NaCl,  0.1 g; CaCl2> 0.1 g; FeClo, 0.02  g; MgS04-7H20, 0.2 g;
CNHJ2S04,  0.7 g; KF^POa, 1.0 g; agar, 15 g;  distilled water, 1000 ml)
containing a parafin hydrocarbon as the sole carbon source was evaluated
as a selective medium for acid-fast bacilli.  Additional  carbon utiliza-
tion studies,  including 15 carbon sources;  acetate, benzoate, pyruvate,
lactate, propionate, malate, oxalate,  citrate,  tartrate,  glycerol,
succinate,  glucose,maltose, lactose,  and mannose, were carried out with
the acid-fast  cultures.   A buffered mineral  medium containing the single
carbon source  under investigation was  used  to culture the acid-fast
bacilli.  Pour plates were inoculated with  stock cultures of the acid-
fast isolates  and growth noted during  a 2 weeks incubation period at 37°C.
                                   20

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Development of an Acid-Fast Staining Procedure  for  Membrane  Filter
Enumeration of Acid-Fast Bacilli

Another approach taken to the problem of selectively  enumerating acid-
fast bacilli in wastewater was the development  of a membrane  filtration
technique.  The general procedure for membrane  filtration of  bacteria
in wastewater, outlined in Standard Method*  (44), was  modified by using
an enrichment broth and medium specific for  acid-fast  bacilli, e.g.,
Middlebrook and Cohn 7H10 agar.  The plates  containing the membranes
were incubated in a humidified incubator at  37°C until the colonies
were visible but not so large that they were easily washed off the fil-
ter when subjected to the staining procedure.   A filter was  removed
from the agar with a forceps and carefully dried above a  flame so as
to prevent charring the filter.  The filters (Type  HA Mi Hi pore  filters,
Mi Hi pore Corp., Bedford, Mass.)  were stained by a  modified  acid-fast
staining procedure.  The solution used in the procedure included 0.5 m£
Brook's carbol fuchsin-dimethylsulfoxide stain  in 20  ml water and 0.5 m£
Brook's malachite green stain containing the decolorizer  (acid-alcohol)
in 20 m£ water; both reagents were obtained  from Curtin Scientific (St.
Louis, Missouri).  The two dye solutions, water for washing  the  filters,
and absolute ethanol were placed in regular  sized petri dishes.  The
filter was immersed in the carbol fuchsin solution  for 30 sec and  then
rinsed completely in water by gently swishing the filter  in  water with
the forceps.  The membrane was decolorized by immersion in  ethanol and
stained in the malachite green solution for  30  sec.  After rinsing in
water, the membrane was allowed to dry and colonies were  observed  under
a dissecting microscope at a magnification of 50 X.

Since no single selective method was completely satisfactory for the
routine isolation of acid-fast bacteria from mixed  microbial populations
such as in wastewaters and feces, methods combining the most satisfactory
pretreatment and culturing techniques of those  studies were evaluated.
Since the samples should be homogenous, large clumps  were dispersed by
the use of a blender.  Samples were then centrifuged  to further separate
particulates from the  liquid suspension.  The centrifuged particles were
resuspended in sterile phosphate buffer and the procedure repeated  if
significant quantities of solid particles were  observed.   The homogeneous
liquid suspension was  then treated with 2.5 percent oxalic acid for  5 to
10 min, followed by neutralization with 2 percent NaOH.  The sample was
then diluted with sterile phosphate buffer prior to application of the
membrane  filter technique.  After 2 to 3 days incubation  on a selective
medium or when visible colonies were evident, the filter was stained
with the modified acid-fast staining procedure and examined for pink
colonies  indicating positive acid-fast bacilli.
                                   21

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                              SECTION V

                        RESULTS AND DISCUSSION


ISOLATES EXAMINED FOR CHLORINE RESISTANCE

Pure cultures of 135 isolates were collected for chlorination  resis-
tance studies.  Although most of these organisms were isolated from
secondary effluents, three bacterial cultures were obtained from chlori-  .
nated tap water and thirteen pure cultures of known species were
obtained from the Department of Microbiology, University of Illinois.
The known stock cultures included the genera:  F£avobact&tx.ujTi, Pieacfoinonai,
S&inatia., MicA.oc.oc.cu:>, Sa^cina, C/itomofaac^eAxxuri,, Stapky£acjOC.c.uA, \McAo-
monobpoM., and S&i&ptomy.  Isolates were also established by sub-
culturing from selected colonies surviving on the assay plates in the
preliminary chlorine screening tests.  It was postulated that these sur-
vivors might have greater resistance to chlorine than the parental isolates

Conditions of isolation and properties of representative isolates are
given in Table 1.   For isolation, this includes the source of each iso-
late, the amount of chlorine added to the effluent and, in some cases,
the free and total  chlorine residuals remaining after 5 or 30 min, the
medium, and temperature of incubation.  The  properties reported in Table 1
are morphology, and Gram reaction.  Many of  the bacteria found after
chlorination of secondary effluents were Gram positive spore  forming rods.
Only a few of these were retained for further study because of the depen-
dence of their spore forming properties on environmental conditions which
makes them generally unsuitable as indicator organisms.  Many different
morphological types of organisms were isolated, primarily at  incubation
temperatures from 20° to 37°C.  Isolates included both Gram positive and
negative rods, cocci, and mycelia with white, orange and yellow pigments.
Organisms were found when as much as 126 mg/i of chlorine  was added to
an effluent sample  to give  25 mg/£ total and 17 mg/£ free chlorine resid-
ual.  Acid-fast bacteria, yeasts  and actinomycetes were the most  unusual
isolates.  The isolation of organisms was conducted over a sufficiently
long period to account for  any seasonal  variation in the wastewater
microbial population.  Considering the number of  isolation experiments
and the  period of examination  it  is  believed that the isolates obtained
were representative of those that might  be commonly  found in  effluents.


FURTHER  EXAMINATION OF  ISOLATES  FROM CHLORINATED WASTEWATER

Although  the  isolates survived various degrees  of secondary effluent
chlorination  {Table 1), most  of  the organisms  isolated  were too sensi-
tive to  chlorine  to be  useful  bioindicators, according  to  the criteria
selected for  this study; that  is,  some degree  of survival  at  concentra-
tions  and contact times  up to  1  mg/Jl free  residual  chlorine for 30 min.
                                    23

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                             Table 1
Conditions of Isolation and Properties of Representative  Isolates
Isolate
No.
5
27
30
32
37
62
67
70
75
82
87
88
Source
AS
AS
AS
AS
AS
AS
AS
AS
TF
TF
TF
TF
Chlorine Free
Added Residual
mg/t mg/l
30.6
42.2
15.2
15.2
44.0
63.0
113.4 2.0
113.4 2.0
126.0 17.0
25.2
25.2
100.8 4.3
ISOLATION
Total
Residual 2
mg/£ Medi a
NA
NA
NA
NA
NA
31.5 SA
NA
ST
25.0 NA
4.6 NA
4.6 TS
19.0 ST
Temp.
°C
20, 37
37
37
37
20
37
20
37
37
20
20
37
PROPERTIES
Morphology Gram Reaction
rust, rods, spores +
yellow rods
oval budding yeast +
6 range mycelium +
oval cocci
yellow rods
yellow rods
curved rods
short rods
round budding yeast +
gold, rods, spores +
yeast, true mycelium +

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                                                      Table  1  (continued)
ro
01
ISOLATION
I sol ate
No.
90
106
114
124
128
132
134
Source
TF
TF
OP
AS
TF
TF
OP
Chlorine Free
Added Residual
mg/£ mg/t
12.6
37.8
30.0
30.0
30.0
30.0
30.0
Total
Residual
mg/t
6.0
24.0
22.7
23.0
25.0
25.0
22.7
Media2
NA
NA
NA
(pH 9)
7H10
NA
7H10
7H10
Temp.
°C
37
37
37
25
10
25
25
PROPERTIES
Morphology Gram Reaction
granular rods
orange mycelium +
large cocci in yellow +
packets
orange rods
yellow coccobacilli
yellow rods, acid fast
thin rods, acid fast
     'Effluents -AS, Activated Sludge; TF, Trickling Filter; OP, Oxidation Pond


     BMedia -  NA, Nutrient Agar; SA, Succinate Agar; TS .Trypti case-soy Agar; ST, Starch; 7H10,  Middlebrook and  Cohn

-------
 There was no significant correlation  found  between the  chlorine resis-
 tance of the isolates  as determined in  chlorine  demand  free water and
 the chlorine dosage used in  the isolation experiments.  This may be
 ascribed to organism protection by clumping and  by extraneous materials
 in the chlorinated effluent.   None of the tap water  isolates nor the
 known stock cultures tested  were sufficiently chlorine-resistant to
 satisfy the initial  screening  criteria.

 Excluding spore-forming  bacilli,  the  isolates which  showed the most
 chlorine resistance were yeasts and acid-fast bacilli which were all
 able to grow on  nutrient agar  as  well as on several  other types of media
 at 37°C.  The general  shape  of the inactiyation  curves  followed a pattern
 frequently reported by various authors, with a lag phase followed by an
 increasing rate  which  finally  leveled off.   However, the length of each
 section of the curve as  well as its rate varied with the chlorine con-
 centration,  the  organism being studied, and other undefined experimental
 conditions,  e.g.,  those  relating  to the growth of the culture in the
 nutrient broth.

 The first promising isolate  found was No. 30, an oval-shaped, asporo-
 geneous, budding yeast that  forms pseudomycelia.  Curves indicating its
 survival to chlorination (Figure  1) show that 0.08 percent of the cells
 survived a free  chlorine residual of  1.0 mg/£ for 20 min while survival
 after 30 min exposure  at 0.1 mg/£ free residual chlorine was greater
 than 80 percent.

 In  studying  Isolate  No.  30, one of the colonies which appeared on the
 assay plate  following  exposure to 1.0 mg/£  free residual chlorine for
 20  min was  subcultured as  Isolate No. 30A.  Studies  on No. 30A showed
 that it was  more resistant to  chlorine than the parent culture, No.  30,
 with nearly  0.2  percent  of the initial inoculum surviving a free chlo-
 rine residual  of 1.0 mg/£  for  30  min  (Figure 2).   However, in later
 experiments  the  chlorine resistance of No.  30A appeared to decrease
 somewhat,  approaching  that of  Isolate No. 30.  This may have been due
 to  an  unstable mutation  to higher resistance or to some function of
 cultivation  of the organism.

 A spherical  budding yeast, Isolate No. 82, was also more resistant to
 chlorine than most of  the bacteria examined (Figure 3);  however, because
 its  chlorine resistance  was much  lower than that of No.  30, organism
 No.  82 was not studied in any  further detail.  Only about 2 percent  of
 the  cells survived a free chlorine residual  of 1.0 mg/& after a 5 min
 exposure.

 Isolate No.  132  is an acid-fast yellow pigmented  rod which showed
 promising chlorine resistance.   Figure 4  shows 63 percent survival
 after  30 min contact of 0.1 mg/t free  residual  chlorine  and 0.05 per-
 cent survival after 15  min of 1.0 mg/£.   Although always remaining at
 quite  a high level, the resistance of this orqanfsm was  more variable
than that of the  other  isolates in comparing different experiments.
                                   26

-------
  o
  3
  (ft

  "c

  u

  I
FIG. I
       0.
              10
            20
   30      40      50


Contact Time, min.
60
RESPONSE OF  ISOLATE  NO. 30 TO  FREE  CHLORINE

RESIDUALS  RANGING FROM O.I TO  1.0 mg/J
                          27

-------
   3
   cn
   c
   0)
   O
   k.
   Q>
   Q.
       0.1
               10
            20     30      40      50


                Contact Time, min.
60
                                                        70
FIG. 2
RESPONSE  OF ISOLATE  NO. 30A TO  FREE  CHLORINE
RESIDUALS RANGING  FROM  O.I  TO  1.0 mg/J?
                          28

-------
  o
  >
  3

  (A
                     20     30     40      50



                        Contact Time, min.
FIG. 3
RESPONSE OF  ISOLATE NO. 82  TO FREE CHLORINE

RESIDUALS  RANGING  FROM 0.1  TO 1.0 mg/J
                         29

-------
   o
   0)
   O
       ai
              10
            20      30     40     90


               Contact Time, min.
60
7Q
FIG.  4
RESPONSE OF  ISOLATE  NO. 132 TO  FREE  CHLORINE
RESIDUALS  RANGING FROM O.I  TO  1.0 mg/J
                          30

-------
The most resistant organism isolated was No.  134,  another acid-fast
bacillus.  To obtain satisfactory survival  curves  for Isolate No.  134,
it was necessary to use higher dosages of chlorine than those used in
experiments with the other isolates (Figure 5).  The lowest  concentra-
tion used was 0.5 mg/£ and 2.0 mg/£ the highest, although 1.5 mg/£ was
the highest dosage applied in most experiments.  In one test,  2  percent
of  the cells survived a free chlorine residual of 2.0 mg/fc  for  67 min.

The free chlorine residuals and contact times necessary to achieve 99.9
percent kill of the four test organisms have been  extrapolated from  the
data in Figures 1, 2, 3, 4, and 5 and are presented for comparison with
data compiled by Berg (50) from chlorination studies on E. call,  adeno-
virus, poliovirus 1, and Coxsackie virus A2 (Figure 6).  The isolates
collected from wastewater in the current study show a definite trend
toward increased chlorine resistance over that of  the traditional  coli-
form indicator.  Isolate Nos.  30, 30A, and 132 show resistance  compa-
rable to or greater than that reported for resistant pathogens such  as
Coxsackie A2 virus.  Isolate No. 134 shows a significantly greater
resistance than the pathogens.  It must be pointed out that  there is
an inherent danger in comparing data presented by  several investigators
collected under possibly dissimilar conditions.  Nevertheless, the data
do suggest that it is possible to obtain vegetative bacteria with suf-
ficient chlorine resistance to make them suitable  as indicators  of the
efficiency of chlorination in destroying resistant pathogens.

Examination of Figure 6 might suggest that Isolate No. 134 could be
too chlorine resistant to be useful as an indicator organism. This  is
not the case for two reasons.  First, it is desirable that an indicator
organism provide a reasonable margin of safety in  indicating the effi-
ciency of chlorination in destroying pathogens.  Secondly, the pathogens
cited in Figure 6 represent only a few of the chlorine resistant patho-
gens found in wastewater and, therefore, might not be representative of
the most chlorine resistant pathogens present in wastewater.  Indeed,
Liu (4) recently showed, in a study of 20 viral pathogens, that  resis-
tance depended on the type of data used to judge resistance.  For
example, the most resistant viruses, using percent survival  at 5 min
contact with 0.5 mg/Jl free chlorine as a judgment criterion, were not
the same as those found to require the longest time to reach 99.99 per-
cent destruction, assuming first order kinetics (4).  In either  case,
Isolate  Nos.  134 and 30A show more resistance to chlorine than  the  most
resistant viral pathogens studied by Liu.  Isolate  Nos. 30 and 132 show
superior survival at 5 min and a similar contact time necessary to
achieve a 99.9 percent destruction.  It should be pointed out that the
experimental conditions used by Liu were different  from  those used in
studying the organisms isolated in the current study.  Direct comparison
of pathogens and the indicator organism under the  same conditions is the
only exact manner in which relative resistance to  chlorine may be
established.
                                   31

-------
   o

       0.1
              10
20      30     40     50

   Contact Time, min.
60
                                                       70
FIG. 5    RESPONSE OF ISOLATE  NO. 134 TO FREE  CHLORINE
         RESIDUALS RANGING FROM 0.5 TO 2.0 mg/jp
                             32

-------
     10
55
£
            Polio  Virus
              Type I
Coxsaekie A2 Virus
  (Clark* SKablflr,
               (Weldenkopf,
                  1958)
          E.Col
            (Butterfield ft
                                                             prg. No
                                                                134
         Adenovirus
          Type 5
             (Clarke, Stevenson
                       Org.No.30
               ft Kobler, 1956)
    0.01
                            10                    100

                             Contact  Tim* (minutes)
                                            1000
       FIG. 6   FREE CHLORINE  RESIDUALS  AND CONTACT TIMES NECESSARY
                FOR 99.9  PERCENT  KILL FOR ISOLATES NO. 134, NO. 30A,
                NO. 132 and  NO. 30 AS WELL AS FOR ORGANISMS COMPILED
                BY BERG (50)
                                  33

-------
 The results  of screening  E.  cjsti ATCC-11229 with  free  residual chlorine
 concentrations of 0.01  to 0.04  mg/£  (Figure 7)  showed  acceptable agree-
 ment with  similar data  collected by  Butterfield et at.  (42) for the same
 E.  coti strain.   The  free chlorine residuals obtained  by Butterfield et at.
 (45)  decreased in the reaction  flasks  from 0.03 to 0.02 and from 0.02 to
 0.01  mg/Jl  after 60 min  while those in  the present study remained constant
 throughout the experiment.   The chlorine resistance of this E. c.oti strain
 is  considerably  less  than that  observed for pathogens  studied by Liu (4)
 or  those compiled by  Berg (50).

 In  the mixed culture  chlorination experiments using Isolate No. 30 and
 E.  coti. ATCC-11229, the percentage survivals of both organisms were less
 than  those observed when  each organism was examined alone.  The reason
 for this discrepancy  was  not readily apparent.  It could have been due
 to  organism  antagonism  in the reaction flask or even growth interference
 in  the agar  plates.

 Results  of experiments  with  Isolate  Nos.  132 and 134  using Tween 80 and
 mixing to  remove  the  effects of possible clumping of these organisms on
 their chlorine resistance showed no significant differences from results
 obtained in  previous  studies when Tween 80 was  not used and mixing was
 not employed.  Thus,  clumping either was not a  factor  in these experiments
 or  was not eliminated when Tween 80 was used in nutrient broth medium
 for the  growth of Isolate Nos.  132 and 134.  Examination of organism
 resistance to  chlorine  under static conditions appeared to be as valid
 as  when  the  tests  were  performed with  mixed reaction systems.

 Several  experiments were  carried out to determine the efficiency of
 chlorination  in destroying Isolate No. 30 in wastewater (Table 2).   Samples
 of  activated  sludge effluent were collected in July 1971 and seeded with
 Isolate  No. 30 and  studied in controlled chlorination experiments.   In
 general, even  though the  chlorine dosages employed in these experiments
 did not  satisfy the total chlorine demand, Isolate No. 30 failed to con-
 sistently  survive  even  5 min contact in 2 of the 3 experiments.  In the
 experiment where  the yeast isolate did exhibit significant survival
 (7/20/71),  the total available  chlorine residual at 5 min contact was
 less  than  that in the experiments where Isolate No.  30 failed to survive.

 Samples of secondary effluent were diluted tenfold,  seeded with Isolate
 No.  30, and studied in  controlled chlorination experiments.  These  experi-
ments were designed to allow use of lower chlorine doses to achieve a
 desired  total chlorine residual  and to provide a situation similar  to
 that which  might be seen in AWT type effluents.   However,  the results
may differ from those obtained in chlorinating actual  AWT effluents since
 the concentrations and types of organic matter and nitrogenous compounds
 in such effluents could  differ from those in diluted secondary wastewater
 effluents.   In addition, the concentration of suspended matter in diluted
 secondary effluent may not be truly representative of AWT effluents.
Survival curves obtained for diluted  wastewater samples are presented
                                   34

-------
 o
 >
 C
 4)
 0)
 Q.
                                        0,02 -*-0,OI mg/i
                                        (Butterfield fllol, 45)
                      O.OE mq/Jt
                                        0,03-»-0,OEmg/X
                                        (Butterfield stall
                              15      20      25

                           Contact Time,  min.

FIG.  7  COMPARISON  OF RESPONSE OF  E, coli ATCC-II229 TO

        FREE  CHLORINE WITH DATA FROM BUTTERFIELD et a[ (45)
                              35

-------
                                                      TABLE  2

                         Chlorination Study of Isolate No. 30  Seeded  in  Secondary  Effluent
CO
cr>



Exp.
Date
1971
77TJ


7/20

7/23



Chlorine
Dosage
(mg/A)

47.1
47.5
48.0
33.8
34.4
4.8
5.2

Apparent
Chlorine
Residuals
(mg/A)

1.60
0.73
1.10
0.10
0.12
1.02
1.35
5 min
Total b
Available
Chlorine
Residuals
(mg/a.)

4.60
8.10
9.30
2.56
2.69
3.46
3.40
Contact Time (min)
15 min


Percent
Survival

0
0
0
73.1
67.7
0
0
Apparent
Chlorine
Residuals
(mgA)

1.30
0.25
0.18
0.10
0.12
0.40
0.70
Total
Available
Chlorine
Residuals
(mgA)

2.60
4.60
7.30
2.54
2.65
1.74
1.50


Percent
Survival

0
0
0
11.7
14.9
0
0
Apparent
Chlorine
Residuals
(mgA)

1.00
0.17
0.18
0.12
0.10
0.25
0.60
30 min
Total
Available
Chlorine
Residuals
(mg/£)

2.20
4.00
0.90
2.49
2.50
1.22
0.96



Percent
Survival

0
0
0
0.5
1.1
0
0
     aFree chlorine residual  determined within 2 min by the DPD method in the presence of combined  chlorine;
      interference by combined chlorine may be present and measured as free chlorine

      Total available chlorine measured by the DPD-potassium iodide method

-------
in Figure 8.   Survival  (Isolate No.  30)  was  measurable at 30 nrin  contact
but varied widely with  survivals of 0.6  and  49.9  percent  for experiment with
2.75 and 1.4 mg/i total available chlorine,  respectively,at 30 min.  Although
not shown in Figure 8,  survival amounted to  0.01  percent  with a total  chlor-
ine residual  of 4.80 mg/£ and a 30 min contact time.

The low survival of Isolate No. 30 in the data of Table 2 and Figure 8 is
not surprising when one considers the high chloramine concentrations
involved in these studies.   High chloramine  concentrations can be an effec-
tive disinfectant with  the contact periods employed with   these data.  In
addition, a transitory  free chlorine residual  most likely will be present
immediately after the addition of chlorine and prior  to the reaction of
chlorine with wastewater organic and inorganic amines. At the high chlor-
ine dosages employed in these experiments a  considerable  level of free
chlorine would be present in the reaction flask for a period of time.


ENUMERATION OF YEASTS IN FECAL MATERIAL  AND  WASTEWATER

Fifty-four fecal samples from healthy human  volunteers were examined  for
total plate count bacteria on nutrient agar  and yeast densities  using
acidified nutrient media, i.e. nutrient  agar or YMA.   The data  (Table  3)
indicates little or no correlation between the number of  organisms deter-
mined by total plate count and the yeasts present in  feces.   The  majority
of the stool samples, at both incubation temperatures (room  ternp^ature,
approximately 25°C, and 37°C), showed 0 to 50 yeasts/g on a wet  basis
(Table 4).  In samples numbered 24 to 54, one-fifth of the stools exam-
ined showed yeast densities in the high  range of 1001 to  10,000/g of
feces.  These latter stool samples were tested using  a more  concentrated
suspension of fecal material than used in samples 1 to 23.  This  appears
to have improved sensitivity.  Approximately 41 percent of samples 1  to
23 showed the presence of yeasts, while 69 percent of samples  24  to 54
showed yeasts with incubation at 37°C.  Use  of room temperature  for
incubation of samples also improved results.  Over 80 percent of the
samples were positive when plated on pour plates incubated at room tem-
perature (approximately 25°C).  When the arithmetic means for room tem-
perature and 37°C data are compared for those samples where  paired data
exists, room temperature data  indicate an advantage over 37°C incubation
by 1,481 to 1,360 yeasts/g of feces.  Of the 28 possible  sets  of data
paired, 16 show greater values  for room temperature incubation and only
six for 37°C, with six giving an equal count at both  temperatures of
incubation.  It has been reported that the pH of the medium,  its com-
position and the temperature of  incubation have a significant effect on
the enumeration of yeasts.  With respect to temperature,   21°C or 25°C
has been suggested to be optimum (51); this is in agreement with the
findings of this study.  Therefore, room temperature with YMA acid
medium at  10 percent or higher  concentration of fecal material seems to
be the technique of choice for  examination of stool samples for yeasts.
From  this  limited study of 54  fecal samples it may be  concluded  that an
                                   37

-------
o
>
c
«
u
        FIG. 8
  12345


Total  Available  Chlorine  Residuals, mg/l



  CHLORINATION STUDY OF ISOLATE NO.  30 SEEDED

  IN DILUTED SECONDARY EFFLUENT
                                                              6
                                  38

-------
CO
                                                    TABLE 3

                           Examination of  Fecal Samples for Total Plate Count and Yeasts
Total1
Plate
Sample Count
Number 37°C
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
33
15
36
18
1.6
5.5
13
102
67
35
0.3
0.25
2
9
1.2
1.6
1.8
4.1
Yeasts2
25°C 37°C
0
0
0
4,000
_
100
0
0
400
0
0
0
1,150
250
0
0
250
100
Samp! e
Number
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
Total1
Plate
Count
37°C
1.8
13
8
29
320
280
2
170
40
65
2.7
61
3.6
6.6
3.9
38
35
25
Yeasts2
25°C 37°C





30
75
620
12
0
140
0
1,040
1,160
0
3
0
25
0
0
200
0
150
-
38
440
12
0
150
0
1,120
-
0
0
0
19
Sample
Number
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
Total1
Plate
Count
37°C
62
11
1.7
1.6
2
18
55
5.2
800
140
470
400
480
170
230
1.7
6.7
330
Yeasts2
25° C 37° C
18
0
11,000
6
1
2,400
72
36
2
12
11,200
5,900
5
10
-
5,000
2,310
1,610
15
1
10,000
5
0
2,230
68
41
0
0
10,000
4,300
290
0
13,500
5,000
2 800
l',600
        1
6
         Number x 10 u per wet gram feces
        2Number per wet gram feces; samples 1 and 2 were plated on acidified potato dextrose  agar;  samples
         3, 7 and 8 were plated on acidified nutrient agar;  all  others were plated on  acidified YMA;
         samples 1-23 were macerated at 1 percent concentrations in phosphate buffer while  4  to 10  percent
         suspensions were used for samples 24-54.

-------
                               TABLE 4

            Statistical Analysis of Fecal Yeast Densities
                                   A.

           Frequency Distribution of Fecal Yeast Densities
Yeast per
gram feces
0
1-50
51-100
101-500
501-1,000
1,001-10,000
>10,000
Samples 1 - 232
37°C
59.1
0.0
9.1
22.7
0.0
9.1
0,0
Samples
Room Temp.4
16.7
40.0
6.7
3.3
3.3
23.3
6.7
24 - 543
37°C
31,0
24.3
3.5
10.3
0.0
20.6
10.3
                                   B.

             Statistical Values for Fecal Yeast Densities
                  Samples 1  - 23        Samplf 24 " 54    All  Samples
                        37°C       Room Temp.4      37°C       37°C
Mean
Median
Percent Positive
300
0.3
40.9
1420
27.5
83.3
1720
37.8
69.0
1141
15
52.9
 Values are percent of total number of samples.
2
 Includes 1      percent dilution of fecal  material  and incubation
 using either nutrient agar, potato dextrose agar,  or YMA media.
3
 Includes 4 to 10 percent dilution of fecal  material  and incubation
 using only YMA medium (pH 3.5-3.9).
Approximately 25°C.
                                   40

-------
encouragingly high percentage of the  population show yeasts in their
stools, and in concentrations up to ICr/g  of  fecal material.

In research complementary to the objectives of this study but not sup-
ported directly by this grant, Panswad (52) studied yeast densities in
raw wastewater and wastewater effluents of the East Side Treatment Plant
of the Urbana and Champaign Sanitary  District. He found that there was
a variation in the number of yeasts detected  at 20° and 37°C.   After 3
days of incubation more yeasts were observed  by colony formation at 37°C
than at 20°C in general but, as incubation time increased, this observa-
tion was reversed, i.e. more yeast colonies were  detected at 20°C.
Mossel at at. (51) also observed that incubation  at 20° to 22°C gave
much higher yeast counts,  Based upon visual  inspection, more rapid
colony development of yeasts occurred at 37°C for no  growth was evident
at the lower temperature (20°C) until after  3 days of incubation.

A mold inhibitor, sodium propionate,  added into YMA medium was found to
inhibit yeasts as well as interfering organisms  in wastewater and was
not useful for that reason.  When 100 ug/mfi,  oxytetracycline was incor-
porated into the medium to inhibit acidophilic bacteria, some degree of
yeast suppression was indicated by a  lower yeast  colony  count.  Thus,
no adjustment other than lowering the pH value of YMA medium was  used
to provide a selective technique for  yeast enumeration.

The yeast densities found in the Urbana and  Champaign Sanitary  District
wastewater samples are presented in Tables 5, 6,  7,  8,  9,  10, and  11.
It should be noted that this treatment plant  is somewhat unique  in  that
the raw wastewater flow is split and  a portion treated by  the activated
sludge process and part by trickling  filters.  This  permits  direct com-
parison of two secondary treatment processes treating the  same  raw
waste.  These data are classified to  show the effects of pretreating
the samples by homogenization  (shaking or blending)  with that of  filtra-
tion  plus shaking.

The pretreating of samples was designed to disrupt any  clumps present 1n
the samples and, therefore, release any yeasts imbedded  in clumps  so
that these yeasts could be enumerated.  Filtering through  cheesecloth, a
common practice 1n studying wastewater microorganisms, would remove many
clumps and any yeasts associated with them,  while vigorously shaking the
samples 25 times or blending for 30 sec should break up  the  clumps.  The
pretreatment appeared to have  Its greatest effect on raw wastewater  and
the least effect on activated sludge  effluent samples.   Using data for
6 days of Incubation, the ratios between filtered and shaken, shaken  only,
and blended samples were 1:5:4, 1:0.9:1, and 1:2.1:1.8 for raw  sewage,
activated sludge, and trickling filter effluents, respectively.   Appar-
ently many yeasts are associated with clumps affected by the pretreatment
1n raw wastewater, fewer 1n trickling filter effluents,  and  very  few,  1f
any,  1n activated sludge effluents.
                                   41

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ro
                                                    TABLE 5

                                   Yeast Densities in Raw Municipal Wastewater
                                        (Acidified YMA Medium at  20°C)
Date
10/05/71
10/12/71
10/21/71
10/27/71
12/07/71
12/14/71
12/16/71
12/17/71
Average
Avg.
Wastewater
Flow
(mgd)
11.9
9.5
8.8
9.1
13.1
14.5
16.4
16.4
Value

Filtered

and
Incubation
4 6
*
370
290
300

930 1
240
260
250

500
400
450
80
500
290
340
400

Shaken
, days
10

*
500
630
100
*
300
450
500
Yeast Count per mil
Shaken
Incubation, days
4 6 10





3500 4000 4300
800 1000 1100
500 800 1000
1400 1900 2100

Blended
Incubation,
4 6





2300 3000
400 500
650 1000
1100 1500


days
10





3200
600
1250
1700
         Enumeration was not possible because of the spreading of mold growth on the medium surface,

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co
                                                   TABLE 6

                                 Yeast  Densities  in Activated Sludge Effluent
                                       (on  Acidified YMA Medium  at 20°C)
Avg.
Wastewate
Flow
Date (mgd)
10/05/71
10/12/71
10/21/71
10/27/71
12/07/71
12/14/71
12/16/71
12/17/71
Average Val
11.9
9.5
8.8
9.7
13.1
14.5
16.4
16.4
ue
Yeast Count per mJl
ir Filtered and Shaken Shaken
Incubation,
4 6
201
95
280
30

180
120
95
180
*
130
310
80
40
400
175
140
220
Blended
days Incubation, days Incubation, days
10 4 6 10 4 6 10

210
400
150
60
630 220 300
215 120 150
200 100 140
310 147 200





* 175 300 600
160 150 170 215
190 100 180 350
140 220 370
        Enumeration was not possible because of the spreading of mold growth  on  the medium surface.

-------
                                          TABLE 7

                         Yeast  Densities  in Trickling Filter Effluent
                               (on  Acidified YMA Medium  at 20°C)
Date
10/05/71
10/12/71
10/21/71
10/27/71
12/07/71
12/14/71
12/16/71
12/17/71
Average
Avg.
Wastewater
Flow
(mgd)
11.9
9.5
8.8
9.7
13.1
14.5
16.4
16.4
Value


Filtered and
Incubation
4 6
330
100
300
95
110
210
130
90
140
*
170
500
160
190
250
200
150
200
Yeast Count per ma
Shaken Shaken
, days Incubation, days
10 4 6 10

200
750
210
270
350 300 600 690
200 180 240 380
200 250 370 400
280 . 240 400 490

Bl ended
Incubation, days
4 6 10





270 550 800
280 350 360
260 350 400
270 420 520
Enumeration was not possible because of the spreading of mold growth on the medium surface.

-------
cn
                                                   TABLE 8

                       Total Bacteria and Coliform Content in Raw Municipal Wastewater
                                             (Incubated at 37°C)
Date
9/19/71
9/23/71
9/30/71
10/21/71
10/27/71
12/14/71
12/16/71
12/17/71
Average Val
Avg.
Flow
(mgd)
10.8
10.3
11.6
8.8
9.7
14.5
16.4
16.4
ue


Total Count x 10 per mH
Filtered and Shaken Shaken Blended
Incubation,
2 4
3.00
2.30
2.30
1.70
0.90
3.70
1.79
1.60
2.00

3.12
2.90
2.30
1.80
6.80
2.60
2.30
2.80
days Incubation, days Incubation, days
6246 246



2.40
1.90
7.40 5.20 9.10 10.80 4.30 6.70 7.20
2.65 5.70 6.10 7.00 4.20 5.00 5.20
2.40 3.60 4.70 5.10 5.00 6.50 7.75
3.00 4.60 6.60 7.60 4.50 6.10 6.70
*
Col i forms
x 10 6
per m£





0.33
0.60
0.15
0.36
        Filtered and shaken  samples

-------
                                          TABLE 9

               Total  Bacteria  and  Coliform Content  in Activated Sludge Effluent
                                     (Incubated at  37°C)
Date
9/19/71
9/23/71
9/30/71
10/21/71
10/27/71
12/14/71
12/16/71
12/17/71
Average
Avg.
Flow
(mgd)
10.8
10.3
11.6
8.8
9.7
14.5
16.4
16.4
Value

Total Count x 10 per m£
Filtered and Shaken Shaken Blended
Incubation, days Incubation, days Incubation, days
24 6246 246
1.00
1.40
1.60
1.80
1.00
1.40
3.20
2.40
1.70

2.30
2.20
2.60 2.80
1.50 1.50
2.80 3.10 2.60 3.20 4.40 2.60 4.70 5.30
4.40 4.60 4.00 4.30 4.50 4.20 5.20 5.80
3.20 3.80 2.80 3.70 4.20 2.70 3.30 4.10
2.60 3.20 3.10 3.70 4.30 3.00 4.40 5.00
*
Coli forms
x 10 6
per ma





0.42
0.96
0.26
0.55
Filtered and shaken  samples

-------
                                           TABLE 10

               Total  Bacteria and  Coliform Content in Trickling Filter Efflent
                                      (Incubated at 37°C)
Date
9/19/71
9/23/71
9/30/71
10/21/71
10/27/71
12/14/71
12/16/71
12/17/71
Average
Avg.
Flow
(mgd)
10.8
10.3
11.6
8.8
9.7
14.5
16.4
16.4
Value

Total Count x 10 per m£
Filtered and Shaken Shaken Blended
Incubation, days Incubation, days Incubation, days
246246 246
1.14
1.74
0.62
0.84
0.85
0.45
0.80
1.50
0.95

2.72
0.90
1.24 1.50
1.20 1.25
0.80 1.20 1.05 1.30 1.40 2.40 5.30 5.50
1.60 1.85 0.90 1.30 1.42 1.34 2.15 2.50
1.75 1.90 0.73 1.08 1.25 1.90 2.40 2.80
1.40 1.60 0.89 1.23 1.35 1.85 3.28 3.60
Coli forms
x 10 6
per m&




0.17
0.19
0.12
0.14
0.15
Filtered and Shaken Samples

-------
 A comparison  of  the  average data of blended samples in Tables 5, 6, and
 7 shows  a  reduction  in number of yeast organisms present following sec-
 ondary treatment, with a greater reduction occurring in the activated
 sludge process than  in the trickling filter treatment.  In Tables 8, 9,
 and  10,  the total bacterial count in samples subjected to various pre-
 treatment  methods -  filtration plus shaking, shaking, and blending alone,
 is compared.  Pretreatment by blending seemed to be the best method of
 sample pretreatment  according to the data presented.  The plate counts
 after blending the sample were higher in general than those after the
 other two  pretreatment methods.  It can be seen from Tables 8, 9, and 10
 that the conform content in raw wastewater, activated sludge, and trick-
 ling filter effluents ranges from 0.15 to 0.60 x 106/m£, 0.26 to 0.96
 x 106/m£,  and 0.12 to 0.19 x 106/m£, respectively.  It is apparent that
 the  activated sludge process used at the Urbana and Champaign Sanitary
 District is less efficient in removing coliform organisms than the trick-
 ling filter treatment.

 A comparison of the  limited data available on yeast densities in waste-
 water as compared to total plate count bacteria and coliforms yields
 approximate ratios for these organisms.  Total plate count bacteria are
 nearly 4000, 13,500, and 7000 times more numerous than yeasts in raw
 wastewater, activated sludge, and trickling filter effluent samples,
 respectively.  Coliforms were approximately 200, 1500, and 290 times more
 prevalent, respectively, in the same samples.  Since comparative data for
 total plate count bacteria, col i forms, and yeasts exist only for filtered
 and  shaken samples which will not reflect organisms associated with large
 clumps,  these ratios should be regarded only as approximations.

 Examination of stool samples and wastewater provided about 47 yeast
 isolates in addition to those obtained from chlorination screening of
 wastewater.  These cultures were randomly selected from assay plates to
 provide  a variety of morphological  types and were by no means inclusive
 of all yeast colonies found on the assay plates,  Identification of yeasts
 is generally based on morphological, physiological, biochemical, cultural
 and other observations,  e.g., shape, size,  maximum and minimum,  as well
 as optimum, temperature for budding and sporulation (53).   Morphologically
 these 47 yeast cultures were categorized into four main groups.   The first
 group, and the most frequently encountered,  were spherical  to oval budding
yeasts forming white smooth colonies that exhibit sedlmented growth 1n
 liquid medium.  The second group of yeasts  were spherical  to oval budding
yeasts forming beige colonies and producing a pellicle in  liquid medium.
The third group of yeasts were elongated to oval budding organisms forming
 creamy white colonies and producing sedimented growth in liquid media,
The last group of yeasts were spherical to  oval budding organisms that
 formed creamy to mucold pink colonies  and yielded sedlmented growth 1n
 liquid media.

Thirteen of these fecal  or wastewater  yeast  isolates were Individually
 prescreened with 0.5 mg/£ free chlorine using chlorlne-demand-free water
under controlled conditions (Table  11).   Four of the cultures tested
                                   48

-------
                             TABLE  11

       Prescreening  for Chlorine  Resistance  of  Yeasts  Isolated^9'
           from Unchlorinated Wastewater Samples  or Stools
Culture
No.
17 T
35 T
2 T
36 T
36 T
53 RT
48
48
15
10
12
44 RT
52

(b)
(b)
(b) .
(b)
(b)
(b)
(c)
(c)
(c)
(c)
(c)
(b)
(c)

5 min
92.5
0.18
91.7
45.8
90.5
76.8
>90
0
63.4
6.0
99.9
52.0
2.6
Time
15 min
4.3
0
58.7
0
3.7
0.9
2.0
0
11.0
0
25.2
0.6
0.1

30 min
0.04
0
0.17
0
4.0
0
0
0
0
0
0.16
0
0
(a)   All  values were determined at 20°C, pH 7, using 0.5 mg/A free
     chlorine; results are expressed in percent survival compared to
     a control

(b)   Cultures isolated from wastewaters

(c)   Cultures  isolated from stools
                                   49

-------
 showed  moderate  to strong resistance to chlorine.  The remainder did not
 survive 30 min contact time.  Representative of each of the four morpho-
 logical-cultural  groups described above were included in these chlorination
 experiments.

 A   heterogeneous  collection of another 24 yeast isolates was  examined in
 a  single mixed culture for chlorine resistance.  Nutrient agar slants
 streaked with pure cultures of yeast were sampled with an inoculating
 loop  and placed  in four flasks containing nutrient broth.  Yeasts placed
 in each of the flasks were of a single morphological type based on the
 morphological classification discussed above.  Broth cultures were grown
 at 25°C for 24 hr on a shaking table.  Following growth, the four cultures
 were  sampled volumetrically, the samples combined, and washed several
 times in sterile  phosphate buffer.  The washed mixed cells were then used
 as the  inoculum  for the chlorination experiment.  A free chlorine dosage
 of 1.05 mg/£ was  applied.  Approximately 1 percent of the total  popula-
 tion  of yeasts  survived after a 5 min contact time.  Surviving colonies
 on YMA  were retained for further study.  This study indicated that the
 mixed population  of yeasts present in wastewater may be sufficiently
 resistant to chlorine to provide a basis for a new indicator group for
 determination of  wastewater chlorination efficiency, as opposed to the
 use of  a single  species or morphological type.


 SELECTIVE TECHNIQUES FOR ENUMERATION OF ACID-FAST BACILLI

 Since the acid-fast characteristics of Isolate Nos. 132 and 134 had
 definitely been established, selective techniques to isolate and to
 enumerate these two cultures were based principally on methods suitable
 for Mt/cobacvte^cum isolation.  The possibility that these isolates could
 be members of the genus Wocotctca was recognized although a limited deter-
 minative study indicated that the cultures belonged to the genus
Isolate No. 132 is a strongly acid-fast bacillus producing yellow, smooth
convex subsurface colonies in pour plates.  In liquid media, such as
nutrient broth, the organism grows homogeneously.  The cells appear to be
pleomorphic  and are arranged singly or in aggregates, large and small.
The optimum growth temperature of this isolate was observed to be 37° C,
although the isolate was also capable of growing at 10°, 20°, 25°, and
45°C.  The isolate was found to be catalase positive but negative for
the hydrolysis  of casein,  gelatin  and starch.   In addition,  the culture
utilized acetate,  succinate,  citrate, malate,  oxalate,  propionate and
pyruvate as a sole carbon  source.

Isolate No. 134, the most chlorine resistant isolate, usually grew as
thin rods forming small branch-like aggregates, exhibiting a moderate
acid-fast characteristic.   It produced irregular buff-colored subsurface
colonies in pour plates.  The optimum growth temperature for this isolate
                                   50

-------
appeared to be 37°C but growth also  occurred  at  10°, 20°, 25°, and 45°C.
Due to the formation of cellular aggregates,  suspensions of this isolate
were particulate in nature rather than  homogeneous.  Addition of Tween 80
to liquid cultures resulted in some  degree  of dispersal of the cell sus-
pensions.  Isolate No.  134 was found to be  capable of  utilizing acetate,
succinate, propionate,  citrate,  malate, oxalate,  and pyruvate as sole
carbon sources.  Both Isolate Nos. 132  and  134 failed  to grow on media
containing benzoate and lactate as the  sole carbon source.  Isolate No.
134 was observed to be catalase positive but  negative  for casein, gelatin,
and starch hydrolysis.   Further physiological  studies  of these two isolates
are needed to provide definitive information  as  to their identity.

A number of studies were carried out in an  effort to develop a rapid, sen-
sitive and selective  technique for  the isolation and  enumeration of these
acid-fast organisms.  These studies  included  examination of methods of
sample pretreatment, study of selective media for acid-fast organisms,
and development of a membrane-filter, acid-fast  staining technique.  The
objective was principally to eliminate  growth of nonacid-fast organisms
in assaying highly contaminated samples such  as  fecal  material and waste-
water.

The alkaline sputum treatment procedure generally used as  a sample pre-
treatment method for clinical identification  of  the tubercle bacilli in
sputum specimens (48) was applied to samples  of  secondary  effluents.
Samples treated with 1  percent sodium hydroxide  showed survival of spore-
formers and a few acid-fast bacilli. To eliminate  growth  of sporeformers
on assay plates, the NaOH dosage was increased to 2,  6,  and  10 percent.
Although growth of sporeformers was  suppressed,  acid-fast  bacilli were
also sensitive to this treatment.

Quaternary ammonium compounds (QAC)  have been used  widely  as disinfectants
in bacteriology laboratories.  Various  QAC were, therefore, examined to
determine if their use as a sample pretreatment  chemical would result  in
suppressing growth of nonacid-fast  contaminants present in wastewater
samples.  Isolate Nos.  132 and 134  were treated with  various QAC at
different concentrations and contact times (Table 12).  Neither  acid-
fast isolate survived treatment with Arquad T-2C-50.   Both organisms
showed some survival to treatment with Armeen C  and Isolate No.  134  sur-
vived 5 min contact with Armeen 12D.  These two  QAC,  i.e.  Armeen  C  and
12D, were examined further to determine how effectively they  suppressed
growth of contaminating wastewater organisms. Trickling filter  effluent
samples were  collected, split, and  portions  treated  separately  with
0.005 percent of each QAC for 5 min  contact.   An untreated portion  of
the effluent was inoculated into Middlebrook and Cohn 7H10 agar  pour
plates.  This untreated sample served as a control.   Treatment of efflu-
ent organisms with Armeen C resulted in a 50 percent  reduction  of organ-
isms growing on 7H10 agar as compared to the control.  Armeen  12D sup-
pressed  growth of 95 percent of the effluent organisms as  compared to
the controls,  A limited number of colonies surviving treatment with
                                   51

-------
                              TABLE 12

              Effect of Selective Pretreatment Methods

                  on Growth of Acid-Fast Isolates
Pretreatment
Chemical and
Contact Time
Arquad T-2C-502
(5 min)

(10 min)

2
Armeen C
(5 min)

(10 min)

Armeen 12D2
(5 min)

(10 min)

Oxalic Acid-NaOH
(5 min)

(5 min)

(30 min)

Colonies Colonies

Concentration

0.005%
Control
0.1%
Control

0.005%
Control
0.1%
Control

0.005%
Control
0.1%
Control

2.5% Oxalic Acid
Control
5.0% Oxalic Acid
Control
5.0% Oxalic Acid
Control
per %
Plate Survival

0 0
190
0 0
90

54 0
190
0 0
90

0 0
190
0 0
90

47 94
50
15 29
50
1040 59
1770
per %
Plate Survival

0 0
180
0 0
250

150 87
180
0 0
250

120 66
180
0 0
250

79 30
260
23 9
260
190 19
990
' M« JJ1 A.L. »A A 1. ~ « _l f*«* t* M ^Ll 1 rt *« M •* u% !.••*.** i i*» ** *j •+ r+ 4* L* *«. f*\**f\l.l 4-t* mf\ f\ llim T M Ti 1 1
experiments.
QAC was dissolved in phosphate buffer (pH 7);  suspensions  were centri-
fuged immediately after the contact time with  QAC and the  cells separa-
ted from the QAC.
                                  52

-------
Armeen 12D were randomly selected  from the  pour  plates and were examined
for acid-fast properties;  3 of 5 colonies studied were found to be acid-
fast positive.  Although both  Isolate  Nos.  132  and  134 showed some resis-
tance to Armeen C, this QAC did not suppress  growth  of wastewater organ-
isms adequately.  While Armeen 12D, on the  other hand, suppressed growth
of nonacid-fast organisms  quite well, Isolate Nos.  132 and 134 were
generally sensitive to this QAC.  Therefore,  the use of QAC as sample
pretreatment agents did not appear promising.

However, since it was found that the QAC dissolved more completely in
ethanol than in water, further experiments  with  QAC  were  carried out
using 40 percent ethanol-QAC solutions.  Low survival of  secondary efflu-
ent organisms was obtained when secondary effluent was treated with
either 0.005 or 0.05 percent Armeen 12D for 5 min  periods.  A few col-
onies examined from the Armeen 12D pretreated assay  plate show acid-
fastness.  Isolate  Nos. 132 and 134 were pretreated with ethanol-Armeen
12D solutions and qualitatively appeared to be able  to withstand this
treatment to some degree.

Use of acid treatment of samples followed by neutralization was studied
as a means for reducing the quantity of nonacid-fast organisms  on pour
plates (Table 12).  Incubation of Isolate Nos.  132  and  134 for 30 min
in 5 percent oxalic acid, followed by neutralization with 4 percent
NaOH, prior to plating in 7H10 agar, gave encouraging results as a sample
pretreatment procedure (Table 12).  Both treatment contact  time and  the
oxalic acid concentration were varied.  Use of  2.5  percent oxal^'  acid
for a contact period of 5 min, followed by neutralization with  2 percent
NaOH, resulted in nearly complete recovery of Isolate No. 132.  A
limited study of  Isolate  Nos. 132 and 134 seeded in secondary  effluent
showed that virtually all of the test organisms  could be recovered  after
the oxalic acid-NaOH treatment  (2.5  percent oxalic acid  for 5 min  contact
time) while only  0.36 percent of the microorganisms  normally  present in
the effluent survived the same treatment.  Therefore, this  pretreatment
method  in isolating acid-fast organisms has been adopted tentatively for
analysis of wastewater samples.

Since other microorganisms, especially sporeformers, may survive  the
oxalic  acid-NaOH  pretreatment,  additional selectivity in the  technique
is necessary  and  could be accomplished through the use of a culture
medium which  is suitable for growth  of only the acid-fast organisms
present  in wastewaters.  A  search  for  an appropriate selective medium
was undertaken  by incorporating various chemotherapeutic agents and dyes
into  the enriched MycobacteJuwn medium, Middlebrook and  Conn 7H10 agar.
Results  of survival  of  Isolate  Nos.  132 and  134 on media incorporating
penicillin,  Eosin-Y,  and malachite green are  presented in Table 13.   Both
cultures showed  good  recoveries when plated  in  a medium  containing Eosin-Y,
However, when a  sample  of  a secondary  effluent was  inoculated on Eosin-Y
medium,  virtually the  same  survival  of effluent organisms was seen as
in  control  plates containing  no Eosin-Y.  Since Isolate  No. 132 failed to
grow  in a medium incorporating  malachite green, no  further study of its
                                    53

-------
                              TABLE 13

     Effect of Selective Media on Growth of Acid-Fast Isolates
Selective
Agent
in Media
Penicillin


Eosin-Y

Malachite
green

Penicillin

Eosin-Y

Penicillin
Eosin-Y

Isolate No. 132

Concentration
500 units /m£ agar
1000 units /mfi, agar
Control
0.005% in agar
Control
0.005% in agar
0.0075% in agar
Control
10 units/mJl agar
Control
0.005% in agar
Control
(10 units /ma agar)
(0.005% 1n agar)
Control
Colonies
per Plate
0
0
1200
380
310
0
0
280
1
150
150
150
0

150
%
Survival
0
0

100

0
0

<0,7

100

0


Isolate No. 134
Colonies
per Plate
4
0.5
1220
130
170
740
630
800
650
700
710
700
710

700
%
Survival
0.4
0.1

76

93
80

93

100

100


Selective agents were incorporated into Middlebrook   and  Cohn 7H10 agar
at concentrations indicated.
                                  54

-------
selectivity was carried out.

Penicillin treatment at concentrations  of 25,  50,  100,  and  250  units/m£
of 7H10 agar, as well  as a combination  of heat and penicillin treatment,
all resulted in the growth of many sporeformers.   Isolate   Nos.  132 and
134 apparently could not survive the  concentrations  of  penicillin used.
Thus, it appears that the use of penicillin  is not feasible as  a selec-
tive agent.

Evaluation of 8 antibiotics with sensitivity discs indicated that, as  a
whole, antibiotics were not suitable  since most inhibited  Isolate  Nos.
132 and 134.  The sulfa drugs, on the other  hand,  showed some promise
since both isolates were observed to  tolerate the  drug  concentrations
impregnated on the discs.  Solutions  of 5 different sulfa  drugs were
therefore incorporated separately into Middlebrook and  Cohn 7H10 agar
and tested against the acid-fast cultures as well  as activated  sludge
effluent.  Results obtained are presented in Table 14.  Isolate No. 132
was generally sensitive to all the sulfa drugs tested.  Since the sulfa
drugs did not dissolve completely in  the phosphate buffer  used, the
actual concentration of the drugs in  the agar was  not precisely known.
The concentration of sulfa drugs in the vicinity of the sensitivity
discs on agar plates depends on the rate of  diffusion of  the  sulfa  drugs
into the media and was, therefore, not precisely known. Thus,  the
results using the sensitivity discs,  and the studies using sulfa drug
suspensions should not be compared.  In summary, the use  of these
chemotherapeutic agents did not appear feasible since the  actual concen-
tration of drugs could not be controlled accurately.

Since the carbon utilization studies  indicated that the acid-fast  isolates
under study were able to grow on simple mineral media with a  simple  carbon
source, it was felt that this knowledge might be  applied  to  the develop-
ment of a selective culture medium for these organisms.  Since  Isolate
Nos. 132 and 134 grew on mineral salt medium containing paraffin as the
sole carbon ^source, this medium was tested for its selectivity  for  acid-
fast bacilli in wastewater samples.  Difficulty was encountered in  dis-
persing the medium in pour plates although its selectivity appeared to
be satisfactory.  Acetate and propionate  were also selected  for use  in
single carbon source media.  These organic compounds were incorporated
into Koser's citrate medium as a replacement for citrate  as the carbon
source.  Selectivity for acid-fast bacilli was demonstrated in  that growth
of sporeformers was suppressed.  Results using raw sewage and acetate
media showed a variety of morphological and colonial forms.  Those cul-
tured on propionate appeared to be morphologically similar to acid-fast
Isolate  Nos. 132 and 134.  Moreover, the selective medium using propio-
nate showed greater inhibition of sporeformers and other nonacid-fast
wastewater organisms than the acetate medium.  Colonies were randomly
picked from propionate medium plates inoculated with raw wastewater and
streaked individually on Middlebrook and Cohn 7H10 agar medium.  Pure
cultures produced on this medium were sampled and tested for acid-fast
                                   55

-------
                                                       TABLE 14



                       Effect of Sulfa Drugs in Selective Media on Growth of Acid-Fast Isolates
en
Apparent Cone.
of Drug
Chemotherapeutic in Water
Agents (mg/£)
No drug present
Kynex


Sulfathiazole


Gantrisin


Sulfamethiozole


Elkosin


Control
1
5
10
1
5
10
1
5
10
1
5
10
1
5
10
Isolate No. 132
Counts/
Plate
72
22
0
0
0
0
0
0
0
0
0
0
0
54
" 0
0
Survival
%

30.6
0
0
0
0
0
0
0
0
0
0
0
75
0
0
Isolate No. 134
Counts/
Plate
290
330
310
330
39
1
0
310
290
290
320
280
13
310
310
310
Survival
%

100
100
100
13.5
0.3
0
100
100
100
100
89.8
4.1
100
100
100
Microorganisms in
Activated Sludge Effluent
Counts/
Plate
310;280
280
160
140
200
120
73
250
150
160
250
130
93
230
210
160
Survival
%

93
52
47
66
40
25
84
51
55
85
44
31
76
71
54

-------
organisms.  Virtually all  colonies  found on  propionate-mineral medium
were acid-fast.

The possibility of using the membrane filtration  technique  after  a
selective pretreatment to determine the presence  of acid-fast bacilli
was investigated.  Determination of acid-fast bacilli  was done by means
of a modified acid-fast staining procedure.   The  result  is  applicable
here because only acid-fast organisms can retain  the primary stain
after the acid-alcohol  decolorization treatment.  Samples  were pre-
treated with oxalic acid, incubated, and neutralized as  described above.

While the resulting data were limited, selective  culturing  of test
samples on membrane filters using a propionate-mineral growth medium
following oxalic add-NaOH pretreatment provided  the potential selec-
tivity and sensitivity necessary to allow the use of acid-fast organisms
as  a possible bioindicator on a routine basis.  The examination  of
several different raw sewage samples indicated that there were signi-
ficant quantities of acid-fast bacilli present.  Counts  of  137 to approx-
imately 500 acid-fast bacilli/nut of raw wastewater were observed  using
this procedure.  Limited studies of wastewater effluent samples  did not
provide reliable results due to considerable quantities  of  finely
divided suspended matter present on the filters.   Several  types  of
colonies were  present including beige, dry-rough colonies, two  types
of creamy smooth colonies, and yellow smooth colonies.  Creamy  and
yellow colonies were found to consist of organisms which were strongly
acid-fast.  While the beige type colonies indicated organisms  which
were definitely acid-fast, they showed a weaker reaction.   The yellow
colonial type appears to be similar to Isolate No. 132.   The beige
variety in pure culture showed a significant percentage of survival
after 30 min contact with 1 mg/Jl free chlorine.  This variety showed
certain resemblances to Isolate No. 134.  The interference  by suspended
matter in enumerating effluent samples may have been due to insufficient
dilution of samples since the suspended matter seemed to show a  limited
degree of positive acid-fast staining.  The literature indicates  that
M?/c0bae£e/uuuri is not Inactivated during conventional wastewater treatment (22,
24,  37) and therefore should be present in the effluent in concentrations
approximating those found in raw sewage.  The dilutions used in  effluent
studies were 100 fold lower than those employed for raw sewage.   As a
result the few assay plates obtained were probably overgrown with acid-
fast organisms.

The combination of a selective pretreatment and a selective culturing
method in the order of oxalic acid-NaOH pretreatment, membrane filtra-
tion,  incubation of the filter on  propionate-mineral medium and  add-
fast staining  of the  filter appears to be promising for the isolation
and enumeration of acid-fast organisms from wastewater, but further
study  is necessary to refine the methods and to more  fully evaluate
its accuracy.
                                    57

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                              SECTION VI

                           ACKNOWLEDGEMENTS
This project was conducted under the auspices of the Environmental Engi-
neering Program of the Department of Civil Engineering, University of
Illinois, Urbana-Champaign Campus.  The helpful suggestions and ideas
of the Environmental Engineering Laboratory personnel, particularly Mr.
Parviz Anrirhor, are gratefully acknowledged.  The data on yeast densities
in wastewater collected by Mr. Thongchai Panswad in a supplementary study,
not directly supported by this grant, provided a valuable input to this
project.  The cooperation of the personnel of the Urbana-Champaign Sani-
tary District is appreciated.

The many suggestions, encouragement, and critical evaluation of the
project data provided by Mr. Cecil W. Chambers, EPA Project Officer,
is gratefully acknowledged.
                                    59

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                             SECTION VII

                              REFERENCES
 1.    Chambers, C. W.,  "Chlorination for Contro] of Bacteria and Viruses
      in Treatment Plant Effluents," Journal Wat&i Pollution Control
               , 43, pp 228-241  (1971).
 2.   Marais, A.  F., Nupen, E. M., Stander, G. J., and Hoffman, J. R. H.,
     "A Comparison of the  Inactivation of E&ch&iichML coli I and Polio-
     virus  in  Polluted and Unpolluted Waters by Chlorination," Inter-
     national  CoKijJeAence on Wote/t, $01 Peace, 3, pp 670-689 (1967).
 3.    Nupen,  E.  M. ,  "The  Isolation of Viruses from Sewage and Treated
      Sewage  Effluents,"  Wat&t Pollution Con&wt, pp 430-435 (1970).

 4.    Liu,  0.  C.,  Seraichekas, H. R., Akin,  E. W., Brashear, D. A., Katy,
      E.  L.,  and Hill, W. J., Jr., "Relative Resistance  of  20 Human Enteric
      Viruses  to Free  Chlorine in Potomac Water," P^oceeciuig^ 13th Sanitary
                           ., University of  Illinois  (1971).
      Kruse",  C.  W., Hsu,  Y.  C. ,  Griffiths,  A.  C.,  and  Stringer,  R.,
      "Halogen Action  on Bacteria,  Viruses,  and Protozoa,"  Rtoceectoigi
      National Specialty Conjjetewce on V  aumii,  Et>chvu,ckia coti, and PA eadomonoi
      avLug
-------
 12.    Favero, M. S., Drake, C. H., and Randall, G. B., "Use of Staphy-
       lococci as Indicators of Swimming Pool Pollution," Pub-tec H&a&tk
               79, pp 61-70 (1964).
13.   Phillips, C. R., "Relative Resistance of Bacterial Spores and
      Vegetative Bacteria to Disinfectants," Bac£e^o£o#tca£ Reucewtt, 16,
      pp 135 (1952).

14.   Brazis, A. R. , Leslie, J. E., Kabler, P. W., and Woodward, R. L.
      "Sporicidal Action of Free Available Chlorine," Special Report to
      Department of Navy, Bureau of Yards and Docks, Project NY 300 010,
      Subproject 6, U. S. Department Health, Education and Welfare,
      Public Health Service, R. A. Taft Sanitary Engineering Center (1957).

15.   Tonney, F. 0., Greer, F. E., and  Danforth, T. F. , "The Minimal
      'Chlorine Death Points1 of Bacteria.  I.  Vegetative Forms," AmeA/ccon
      Journal Piibtic UuJLth, IS, pp 1259 (1928).

16.   Stringer, R. , and Kruse," C. W., "Amoebic Cysticidal Properties of
      Halogens in Water," ?nocjt£nte.ction, pp 635-681, American Society
      of Civil Engineers, New York (1970).

18.   Moore, E. W., "Fundamentals of Chlorination of Sewage and Waste,"
      Watesi and Sewage, WOA/W, 98, No. 3, pp 130 (1951).

19.   Kapoor, S. K., A Critique on Disinfection of Drinking Water,"
      M. S. Thesis, University of Illinois, Urbana (1969).

20.   Chang, S. L., and Kabler, P. W., "Detection of Cysts of Endamoeba
      hy&toh/tica in Tap Water by Use of a Membrane Filter," Ametxcon
      Journal Hyglwe,, 64,  pp 170-180 (1956).

21.   Jensen, K. A., and Jensen, K.  E., "Occurrence of Tubercle Bacilli
      in Sewage and Experiments on Sterilization of Tubercle Bacilli
      Containing Sewage with Chlorine," Ac&x JubeAcuJtoAta. Sc.andana.vJ,c.a.,
      14,  pp 125 (1940).

22.   Pramer, D., Heukelekian,  H., and Ragotzkie, R. A., "Survival of
      Tubercle Bacilli in Various Sewage Treatment Processes," Piibtic.
      He.aJtth tepavte,  65, pp 851-859 (1950).

23.   Grabow, W. 0.  K. ,  Grabow, N.  A., and Burger,  J. S., "The Bactericidal
      Effect of Lime Flocculati on/Flotation as a Primary Unit Process in a
      Multiple System for the Advanced Purification of Sewage Works Effluent,"
      Wote* Jteaeotc/t,  3,  No.  12, pp  943 (1969).
                                    62

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24.    Musehold,  P., Atbexxten a.  d.  KcuAeLichw  GeAundk<amt,  22,  pp  56
      (1900).

25.    Kabler,  P.  W., "Removal of Pathogenic  Microorganisms  by  Sewage
      Treatment Processes,"  Swage. and lndu&fru,at WatteA,  31,  No.  12,
      pp 1373 (1959).

26,    Greenberg, A. E., and Kupka, E., "Tuberculosis Transmission  by
      Waste Waters - A Review,"  Swage, and Indus>&u.at Wa&teA,  29,  No.  5,
      pp 524 (1957).

27.    Cooke, W.  B., "The Enumeration of Yeast Populations  in a Sewage
      Treatment Plant," Mt/ao£og-ai, 57, pp 696 (1965).
28.   Skinner, C. E., Emmons, C. W., and Tsuchiya, H.  M. ,
      Mo£d, VaoitA, and Aattnomycet&i, 2nd ed., John Wiley and Sons,
      New York (1947).

29.   Benham, R. W., and Hopkins, A. W., "Yeastlike  Fungi Found on the
      Skin and in the Intestines of Normal Subjects," Aich. VeAmatoi
      SypkUol., 2$, pp 532 (1933).

30.   Cooke, W. B., Phaff, H. J., Miller, M. W., Shifrine, M. , and
      Knapp, E. P., "Yeasts in Polluted Water and Sewage," Myc.o&)g
-------
37.   Muller, 6., "Tuberkel bacterien ImSchlamm Median is ch - Biologisch
      Arbeitende Abwasser reinigungsanlagen," Sta.dteJkygle.nn, 5, pp 46-47
      (1959).

38.   Palin, A. T., "The determination of Free and Combined Chlorine in
      Water by the Use of Di ethyl -p-phenylene Diamine," Joutnat Amvu.can
                  M&ocia£ion, 49, pp 873 (1957).
39.   Adams, D. B., Carter, J. M., Jackson, D. H., and Ogelby, J. W.,
      "Determination of Trace Quantities of Chlorine, Chlorine Dioxide,
      Chlorite, and Chloramines In Water," P/toaeedoia* Society
                and Examination, 15, Part 2, pp 117 (1966).
40.   Bjorklund, J. G., and Rand, M. C., "Determination of Free Residual
      Chlorine in Water by Para-Aminodiethlaniline," Jousui&t American
            Wo4.fe4 Association, 60, pp 608 (1968).
41.   Lishka, R. J., McFarren, E. F., and Parker, J. H., "Ferrous Method
      for Free Available Chlorine, Monochloramine, Dichloramine, and
      Nitrogen Trichloride," Mite*. CkloJLine, (Retidu&t) No. 1, No. 35,
      U. S. Department Health, Education and Welfare, PHS, Appendix C,
      60 (1969).

42.   Marks, H. C., "Residual Chlorine by Amperometric Titration," Joutnat
      Wew England WateJi W^feA faAociation, 66, No. 1 , pp 1 (1952).
43.   Chambers, C. W., Project Office, Biological Treatment Research
      Program, National Environmental Research Center, Cincinnati, Ohio,
      Personal Communication (1970).
44.   Standard Methods Ion the, Examination orf W&te/i and WaAteiaateA, 13th
      ed., American Public Health Association, American Water Works
      Association, Water Pollution Control Federation, New York (1971).

45.   Butterfleld, C. T., Wattle, E., Megregian, S., and Chambers, C. W.,
      "Influence of pH and Temperature on the Survival of Conforms and
      Enteric Pathogens when Exposed to Free chlorine," Public. He&Ztk
      Rcpcwt, 58, No. 51, pp 1837 (1943).

46.   Megregian, S., "The Preparation of Chlorine- Demand- Free Water,"
      PubUc He.a£tk Ktpovt,  63, No.  5, pp 137 (1948).
47.   Lodder, J., ed., The, yzaAte:  A Taxonomy Study,  2nd ed., Delft,
      The Netherlands (1970).
48.   Allen, B. W., and Baker, F. G., Mt/cobacte^ca Isolation
      cation,  and Sin&ittvity Testing, Butterworths and Co., Ltd.,
      London (1968).
                                    64

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49.   David, H.  L., Chief,  Mycobacteriology Unit,  Center for Disease
      Control, Atlanta, Georgia,  Personal  Communication (1971).

50.   Berg, G.,  "Virus Transmission by the Water Vehicle,   III.   Removal
      of Viruses by Water Treatment Procedures," Heo&tfi LoboAotoJur
      Science, 3,  No.  3, pp 170 (1966).

51.   Mossel, D. A. A., Visser, M. , and Mengerink, W.  H. J., "A Comparison
      of Media for the Enumeration  of Moulds and Yeasts 1n Foods and
      Beverages," Laboxatony PMLvUte., 11, pp 109 (1962).
52.   Panswad, T., "Occurrence of Yeasts 1n Municipal Wastewater Treatment,"
      M. S. Special Problem, University of Illinois, Department of Civil
      Engineering, Urbana (1972).
53.   Prescott, S. C., and Dunn, C. G., InduAtMaJi fAicnobAology,  3rd ed.,
      McGraw-Hill, New York (1959).
                                     65

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                             SECTION VIII

                       PUBLICATIONS AND PATENTS
Greening, E. 0., "Microblal Indicators for the Biological  Quality of
Treated Wastewater Effluents," M.S. thesis, Department of Civil Engineering,
University of Illinois at Urbana, 1971.

Greening, E. 0., Lee, S. H., and Engelbrecht, R.  S., "Microbial Indicators
for the Biological Quality of Chlorinated Wastewater Effluents," presented
at 72nd Annual Meeting of American Society for Microbiology, April 28, 1972.
                                   67

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SELECTED WATER
RESOURCES ABSTRACTS

INPUT TRANSACTION FORM
    Report No.
                      w
           NEW MICROBIAL  INDICATORS OF WASTEWATER
           CHLOR1NATION EFFICIENCY
           Engelbrecht, R.  S.,  Foster, D. H., Greening, E. 0.,
           and  Lee,  S. H.
          Department  of C1v1l  Engineering  (Environmental
          Engineering) at  Urbana-Champaign, University of
          Illinois, Urbana,  Illinois
                      5.  Report Date

                      6.  ' ' '     .   .

                      «.  Petforaiuz Organbttion
                         Report No.
                          17060 EYZ

                      13. Typ* W Report and
                         Ptrtad Coveted
                     1BB043/21ASS/05
           Environmental Protection Agency report number,
           EPA-670/2-73-082,  February 1974.
          The coHform group of Indicator organisms has a relatively low resistance to
chlorine when compared to pathogens such as enteric viruses and protozoan cysts.  Con-
sequently, an effort has been Initiated to find a new chlorine resistant b1o1nd1cator
of wastewater chloHnatlon efficiency.  Organisms surviving chlorlnatlon of wastewater
effluents to a free chlorine residual were collected for study by plating on various
growth media.  This procedure provided 135 chlorine resistant Isolates for further
examination.  A yeast and two different add-fast bacilli were found to be resistant
to chlorlnatlon 1n the range considered necessary for the 1nact1vat1on of pathogens,
Including viruses,  One add-fast bacillus survived 2.0 mg/£ free chlorine for 67 m1n
while the other survived 1.0 mg/£ free chlorine for 15 m1n.  The yeast resisted 1,0
mg/£ free chlorine for 20 m1n.  In comparison, a pure culture of E. cote failed to
survive 5 m1n contact with 0.03 mg/l free chlorine.  Add-fast staining of colonies on
membrane filters  Incubated on mineral-proplonate medium, following sample pretreatment
with oxalic add  and NaOH provided a selective assay technique for add-fast organisms.
Significant quantities of yeasts and add-fast organisms were found 1n wastewater
effluents and yeasts have been Isolated from stools.  The chlorine resistance and other
characteristics of the yeasts and add-fast bacilli under study suggest that they show
promise as b1o1nd1cators for wastewater chlorlnatlon efficiency for the more chlorine
resistant pathogens.
 11a. Descriptors                                         *              *
          B1o1nd1cators , bacteria, conforms, yeasts , chlorlnatlon , wastewater
treatment*, viruses, public health, water reuse, activated sludge, trickling filters,
resistance*, sewage bacteria


 17b. Identifiers

          Enteric viruses, chlorine resistance, pour plates, add-fast bacilli
 17c. COWRR Field & Group   05A, 05D
                                                    WASHINGTON. D. C, 2024O
          David H. Foster
'"»•••> Univ.  of Illinois, Urbana. Illinois
 «U.S. GOVERNMENT PRINTING OFFICE: 1974  546-318/336  1-3

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