<>EPA
United States     Industrial Environmental Research  EPA-600/7-79-108
Environmental Protection  Laboratory          April 1979
Agency        Research Triangle Park NC 27711
Studies of Dust Cake
Formation and Structure
in Fabric Filtration:
Second Year

Interagency
Energy/Environment
R&D Program  Report

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                  RESEARCH REPORTING SERIES


Research reports of the Office of Research and Development, U.S. Environmental
Protection Agency, have been grouped into nine series These nine broad cate-
gories were established to facilitate further development and application of en-
vironmental technology. Elimination  of  traditional grouping was consciously
planned to foster technology transfer and a maximum interface in related fields.
The nine series are:

    1. Environmental Health Effects Research

    2. Environmental Protection Technology

    3. Ecological Research

    4. Environmental Monitoring

    5. Socioeconomic Environmental Studies

    6. Scientific and Technical Assessment Reports (STAR)

    7. Interagency Energy-Environment Research and Development

    8. "Special" Reports

    9. Miscellaneous Reports

This report has been assigned to the INTERAGENCY ENERGY-ENVIRONMENT
RESEARCH AND  DEVELOPMENT series. Reports in this series result from the
effort funded under the 17-agency  Federal Energy/Environment Research and
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                                       EPA-600/7-79-108

                                                 April  1979
 Studies  of Dust Cake Formation
and  Structure in Fabric  Filtration:
                 Second  Year
                         by

            Bernard Miller, George Lamb, Peter Costanza,
          George Harriott, Janet Dunbar, and Michael Mokricki

                  Textile Research Institute
                      P.O. Box 625
                 Princeton, New Jersey 08540
                    Grant No. R804926
                Program Element No. EHE624A
               EPA Project Officer: James H. Turner

            Industrial Environmental Research Laboratory
              Office of Energy, Minerals, and Industry
               Research Triangle Park, NC 27711
                      Prepared for

            U.S. ENVIRONMENTAL PROTECTION AGENCY
               Office of Research and Development
                   Washington, DC 20460

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                             ABSTRACT


       This report describes progress toward the project objective:
to explain changes in the performance of fabric filters on the basis
of changes in the structure of the deposited dust cake.  Whether im-
proved performance (that is, greater collection efficiency with lower
pressure drop) is obtained by imposition of electric fields, by mak-
ing the filter fabric out of fibers having modified geometries, or
by varying fabric construction, the improvement is associated with
deposition of the dust close to the upstream region of the filter
rather than deep within it.  (In this work the dust cake is under-
stood to include dust that penetrates into the filter fabric.)

       An electric field applied to a fabric filter is more effec-
tive in reducing pressure drop if the fabric has loose fibers at the
surface.  When a dust cake is formed on such a fabric in the presence
of a field, photographs of the cake surface show heavy deposition on
protruding surface fibers.  In contrast, after filtration without a
field these fibers are bare, and the mass of dust penetrating into
the fabric is greater.  Thus the combination of applied field and
protruding fibers results in reduced penetration into the filter
and concomitant pressure drop reduction.

       Without an imposed field, using fibers with deeply lobed ra-
ther than round cross sections results in improved performance, and
the associated increase in upstream capture is attributed to induced
localized fields due to the collection of the naturally charged
aerosol particles.  Using the principles evolved in bur earlier
studies of the effects of fiber geometry on performance, layered
filters have been prepared having upstream and downstream layers
made of fibers differing in linear density which give better per-
formance than homogeneous fabrics.  These fiber and fabric modifi-
cations that improve capture in the upstream fabric layers also
allow more effective cleaning (that is, less long-term dust reten-
tion) , which accounts for at least part of the reduction in pressure
drop.

       In general, it appears that collection closer to the upstream
filter surface is associated with higher overall collection effi-
ciency, easier cleaning, and lower pressure drop.

       This report is submitted in fulfillment of Grant No. R804926-2
by Textile Research Institute under the sponsorship of the U.S. En-
vironmental Protection Agency.   This report covers a period from
December 20,  1977 to December 19, 1978, and work was completed in
December 1978.
                                   11

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                              CONTENTS
                                                                 Page
  Abstract                                                        ii
  Figures                                                         iv
  Tables                                                           v

  Acknowledgments                                                 vi

  I.  INTRODUCTION 	   1

 II.  SUMMARY AND CONCLUSIONS	   2

III.  EFFECTS OF EXTERNALLY-APPLIED ELECTRIC FIELDS	   4

      A.  MICROPERMEABILITY SCANNER	   4

      B.  MEASUREMENTS OF CAKE DEPTH	   8

      C.  NEW EMBEDDING PROCEDURE FOR CAKE CROSS-SECTIONING.  .  .  12

      D.  PHOTOGRAPHIC ANALYSIS OF DUST CAKES	14

      E.  EFFECT OF FABRIC STRUCTURE 	  14

      p.  STUDIES OF DENDRITE FORMATION	21

      G.  EFFECT OF CORONA	23


 IV.  EFFECTS OF FIBER GEOMETRY	26

      A.  MECHANISM OF PRESSURE DROP REDUCTION WITH
          TRILOBAL FIBER FILTERS  	  26

      B.  X AND Y-SHAPED FIBERS	26

      C.  COMPOSITE FILTERS	33

          1.  Initial Cycles	33
          2.  Conditioned Fabrics	34


  V.  REFERENCES	38
                                   ill

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                            FIGURES

Number                                                         2*2*.

   1   Micropermeability scanner                                 5
   2   Scan of permeability (expressed as pressure drop at
       constant air flow) for dust cakes deposited at 0, 2,
       4, and 6 kV/cm                                            7
   3   Fractional collection on layers of electrified
       layered filters                                           9
   4   Capture efficiency of each layer of filters in
       Figure 3                                                  9
   5   Upstream surfaces of layers of nonwoven fabrics of
       Figure 3 used to filter flyash at 0 (left) and 2  (right)
       kV/cm                                                    1°
   6   Upstream surfaces of layers of nonwoven fabrics of
       Figure 3 used to filter flyash at 4 (left) and 6
       (right) kV/cm                                            H
   7   Photomicrograph of cross section through commercial
       needled PET filter fabric and dust cake                  13
   8   Cross section through dust-coated fabric prepared by
       embedding procedure                                      15
   9   Photographs of the surfaces of the dust-laden filters
       in Figure 8                                              ^
  10   Effect of fabric upstream surface structure on
       pressure drop ratio                                      19
  11   Cross section through the fabric used for Figure 9
       but with no dust                                         20
  12   Basic structural configurations for flyash deposits
       (schematic)                                              22
  13   Collection of charged particles on  (a) charged and
       (b) neutral surfaces (schematic)                         22
  14   Micrographs of flyash collected on trilobal polyester
       fibers                                                   22
  15   Variation of calculated surface field with applied
       voltage for wires of different diameters                 24
  16   Flyash retained by layered filters as conditioning
       proceeds                                                 27
  17   SEM cross sections of trilobal fibers                    29
  18   SEM cross sections of acetate fibers                     30

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                         Figures (con.)

Number                                                         Page

  19   Comparison of pressure drop with fabrics made of
       I, Y, and X-shaped acetate,  trilobal PET (A), and
       round PET Co) fibers                                     32

  20   Comparison of penetration (1-efficiency) with fabrics
       made of I, Y, and X-shaped acetate, trilobal PET (A),
       and round PET (o) fibers                     '            32

  21   Performance curves for the fabrics in Figures 19
       and 20                                                   32

  22   Changes in pressure drop during conditioning of
       composite PET filters                                    35

  23   Changes in pressure drop during the 20th cycle for
       composite PET filters                                    35

  24   Pressure drop across composite vinyon-bonded PET
       filters having varying proportions of 3 and 6-denier
       fibers in two layers                                     37

  25   Penetration through the composite filters of Figure 24   37

  26   Residual dust after cleaning the filters of Figure 24    37
                             TABLES

Number                                                         Pa3e

   1    Efficiencies  and Pressure Drop  Changes  Due to
       Electric Field of  2  kV/cm Applied  to Woven and
       Nonwoven Glass and PET  Fabrics                            17

   2    Properties of Felts  Made from Acetate Fibers with
       Various Cross Sections                                    31

   3    Composite Filters  Made  of 3 and 6-Denier  Trilobal
       Polyester Fibers                                          33

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                           ACKNOWLEDGMENTS

      The authors would like to express their appreciation to
Dr, James H. Turner of the Environmental Protection Agency for
his advice and encouragement throughout the period of this research.
They would also like to thank Mr. Harold W. Lambert and Mr. Harry
Buvel of TRI for their invaluable work on apparatus, Mr. John P.
Hession for his assistance with microscopy, and Dr. Harriet G.
Heilweil for her help with reports.

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                           SECTION I


                          INTRODUCTION
      The following report describes work that was done in the
second year of a three-year program and must, therefore, be read
as a continuation of the report issued a year earlier [4].  Simi-
larly/ some of the conclusions drawn are not final but relate to
studies which continue and will be discussed further in the final,
third-year report.

      The main object of the work is to find explanations for
observed changes in -Filtration performance that result from cer-
tain modifications QJ. conventional fabric filtration technology.
One such modification is the use of fibers having different geo-
metric properties from those of fibers commonly used in filter
fabrics (cross-sectional shape, surface roughness, linear density,
etc.).  Another is the application of electric fields to the fa-
brics.  A third is the use of creped fabrics.

      In each case some of the improvements in performance, which
have taken the form of increased capture efficiency, reduced pres-
sure drop, or both, appear to coincide with changes in dust cake
characteristics.  Therefore, a primary goal of the present work
is the identification of features of the dust cake or of the fabric-
dust system which may explain the observed changes in performance.
A second goal is to use this information as a basis for the de-
sign of improved filter fabrics or systems.

      The term "dust cake" tends to mislead because it conveys
the image of a dust layer in contact with but separate from the
filter fabric.  In fact, there is considerable deposition within
the fabric, so that a study of dust cake structure is really a
study of the dust-laden surface layers of the fabric.

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                            SECTION II


                     SUMMARY AND CONCLUSIONS


     Studies of the local permeability of dust cakes formed with
externally applied electric fields have shown that light and dark
bands observed in top-view photographs are not due to uneven depos-
ition across the fabric and therefore cannot be the basis for an
explanation of the reduced pressure drop produced by a field.  On
the other hand, measurements of the depth of penetration of the dust
into the fabric indicate that the effect of the electric field is
to concentrate the dust accumulation in the upstream layers of the
fabric, allowing less to penetrate deeper inside.

     Study of the vertical cross-sectional structure of the dust
cake as modified by an electric field was attempted by a photogra-
phic approach.  An embedding procedure was developed which at first
appeared to preserve the cake intact and to allow cross-sectioning
of cake and filter fabric.  It later became apparent, however, that
the embedding process disturbs the features which are of greatest
interest, namely the deposits on the surface fibers.

     On the other hand, examination of top-view photographs of the
filter-cake surfaces has revealed features indicating that reduction
in pressure drop due to an electric field depends on fabric construc-
tion.  Heavy deposition on fibers protruding from the fabric surface
is evident in the photographs, suggesting that the shift of the dust
deposit upstream is extreme.  It has also been found that pressure
drop is reduced by the electric field more or less depending on whe-
ther or not the fabric has a surface layer of loose fibers.

     The question of whether, in addition to the changes in the posi-
tion of the dust cake, there also occur microscopic changes at the
single fiber level when an electric field is applied has been ad-
dressed by photographic studies of dust captured on single fibers.
Initial results indicate that, whereas in the absence of an electric
field dendrites tend to form, a field causes formation of a more uni-
form, nondendritic deposit.  This finding is consistent with the
lower pressure drop developed with a field.

     Work was also continued on the effects of fabric or fiber geo-
metry on dust cake formation in the absence of fields.  The effects
of fiber geometry were further examined by measuring dust deposition
in different layers of fabrics made of round or trilobal fibers.
The previous report presented data showing how when these fabrics
are new  (i.e., at the first cycle), dust tends to be captured more
efficiently in the upstream layers.  The amount of dust in the vari-
ous layers of the filters after a number of conditioning cycles has
now been measured, and the fabric made of trilobal fibers retains
less dust in all layers.  It is assumed that by favoring capture in
the upstream layers, trilobal fibers also favor easier cleaning.

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This results in less long-term dust retention and explains the lower
pressure drops measured in the past with fabrics made of trilobal ra-
ther than round fibers.

     Similar results were obtained with fabrics made of fibers with
"Y," "X,"or "I" cross sections which had deeper and/or more lobes
than the trilobal fibers used before.  In each case, the performance,
gauged by both penetration and cake resistance, was improved over
the shallow-lobed trilobal fibers.  Since this finding fits a theor-
etical prediction of better capture efficiency by many and deep-lobed
fibers in an electric field, the hypothesis is that the improved
performance is due to electric charges on the aerosol which when de-
posited in the fabric, generate an electric field.

     Finally the stu ,y of composite fabrics has continued.  It has
long been felt that better filters,filters that are durable as well
as effective and economical, could be produced by fairly simple modi-
fications of fabric construction.  An example is forming the fabric
in dissimilar layers.  Measurements on fabrics made of layers of rel-
atively fine and coarse fibers (3 and 6-denier) over a large number
(^50) of conditioning cycles gave several interesting results.  As
conditioning progresses, the relative ranking of different fabrics
with respect to performance changes.  The first result, therefore,
is that in studies of this type, it is important to insure complete
conditioning before drawing conclusions about relative performance.
The second result is that the performance of such composite fabrics
is quite different from what might be expected from knowledge of the
performance of the component layers.  There is thus a good potential
for designing improved filter fabrics by this type of combination.
The third result is that the differences in performance appear to be
associated with the amount of dust retained in the fabric.

     The work described in this report indicates that external appli-
cation of electric fields, use of lobed fibers, and use of composite
fabrics have a common effect:  modifications that cause dust to be
deposited closer to the upstream surface of the fabric bring about
improvements in both efficiency and pressure drop.

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                            SECTION III

          EFFECTS OF EXTERNALLY-APPLIED ELECTRIC FIELDS


      The largest improvements in fabric filtration performance
have been obtained by the application of electric fields.  Effects
on capture efficiency have been reported by a number of workers
11,2,3,], but few commercial filter units designed to take advan-
tage of such improved efficiency have appeared on the market.  Lit-
tle has been reported regarding reduction in pressure drop accompa-
nying the application of electric fields, though this is perhaps
more important than increased efficiency since it has potential
for lowering the cost of filtration by fabrics.  This may make
electrically stimulated fabric filtration (ESFF) commercially attrac-
tive where improvements in efficiency alone might not.  The mechan-
isms whereby efficiencies increase in the presence of electric
fields have received a great deal of attention and are well under-
stood, at least for clean filters.  The cause of a reduction in
pressure drop can only be conjectured at this time, though it is
obviously related to some change in the dust cake structure.  The
exact nature of that change, however, is not known, and a better
understanding of it was the aim of the studies described in the
following section.


A. MICROPERMEABILITY SCANNER

      In the preceding report [4] photographic evidence was given
of nonuniformity of distribution in dust cakes formed on patch fil-
ters under the influence of electric fields.  In most cases there
appeared to be different amounts of dust deposited on or near the
electrode wires than between them, and this suggested a possible
mechanism for the pressure drop reduction effect with ESFF.  If
the electric field causes an uneven dust deposit to form, then the
resistance to gas flow through the dust cake would be reduced,
since (by analogy with electric resistance)  if R is the overall
resistance to flow and R^ is the resistance of an element of dust-
cake area, the relationship would be of the form
                    R = [Z  j    ,


where R becomes smaller with increasingly dissimilar R^.

      In order to check this hypothesis, an apparatus was devised
for measuring the permeability of the dust cake at a number of
small areas on a patch filter.  Of several designs tried, the one
shown in Figure 1 was found to be the most satisfactory.  After
the dust cake has formed, the dust- laden fabric is carefully
clamped between the perforated plates A and B.  As shown in

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 (a)



    r.





A  -H


 B-






(b)
                       Manometer

                                           «- Dust cake

                                              Fabric
          Air flow
                 Brass tube
                      A- Dust cake
     B
                      Electrode wires
      (d)
                         ...   ..  Pressure
                         Needle regulator
                          valve
        Filter mount
                              =5=
                              Manometer
                                            Air

                                           supply
Figure  1.  Micropermeability  scanner:   a)  side view  of filter

  mount;   b)  detail;   c) top  view;   d) general layout.

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  Figure la,  the pins  C and D have the double  function of  insuring
  that the  holes in the plates will be aligned,  and  also that, when
  the plates  are placed on the fabric,  there will  be no lateral
  motion that could disturb the cake in the small  areas to be
  measured.   As  shown  in the detail,  Figure Ib,  the  hole on the
  cake side is slightly larger than its counterpart  on the downstream
  side of the fabric.   A brass tube,  which has a sliding fit into
  the cake-side  hole,  is placed in the hole and  pressed against  the
  fabric, making a  tight seal.   A steady stream  of air passes down
  the tube  and through the small area (o.6-mm diameter) of  dust cake
  within the  seal.   The pressure drop across the dust cake is mea-
  sured by  the manometer (Figure  Id).   The holes  in plates A and B
  are arranged so as to scan across the patch  at positions on the
  wire electrodes,  and at 1/4,  1/2,  and 3/4 of the distance between
  them,  as  shown in Figure Ic.

         A  sample of polyester (PET)  needled felt  was fitted with
copper wire  electrodes.   The felt was  a commercial  filter fabric
 (the patch was  cut from a purchased  bag) having a central scrim
and  was composed of 9-denier polyester fibers compacted into a
felt structure  by  a needling process.   It is  listed in Table I
as the Carborundum PET nonwoven.   The  electrode wires were
threaded just below the upstream surface by means of a sewing
needle.  Figure Ic shows how the electrodes were  coupled  to the
power supply in this  and all subsequent measurements involving
filter patches  fitted with electrodes.   The filter  was conditioned
in the patch filter apparatus  with applied fields of 0, 2,  4, and
6 kV/cm.  The last cycle was interrupted before cleaning  and the
fabric lifted out  with the dust cake.   The cake was then  scanned
by making pressure-drop measurements at holes across the  filter,
according to the procedure outlined  above.  The flow of air in  the
tube was adjusted  to  be equal  to the  face velocity  during formation
of the dust  cake.   Consequently,  the pressure drops measured could
be directly  compared  with the  final  pressure  drop APf obtained  with
the  particular  dust cake.   The  results  are plotted  in Figure 2.
The  four curves  are permeability scans  for cakes  formed at the  four
electric field  strengths.   The  pressure  drops measured in each  scan
can  be  seen  to  correspond well  with  the  final pressure drops APf
measured as  the  cake  was  being  formed,  given  4n Figure 2.

       The results  in Figure  2  show no  particular pattern  of cake
permeability with  respect  to position  relative  to the electrodes.
Some  fluctuations  in  cake  permeability  are seen,  but these  do not
coincide with the  electrode position and are  not  introduced by  the
field  since  they are  present even when  no voltage is applied.
Therefore,  the lower  pressure drop is  the result of  a general
increase in permeability  of the  entire cake.   In  fact,  these
results may be taken  as proof that the  hypothesis of pressure-drop
reduction by unbalanced permeabilities  is invalid.   The patterns
of apparently uneven  distribution  seen previously [4] still remain
to be explained, but  they  appear  to be  irrelevant to the  question
of pressure-drop reduction by ESFF.

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   PRESSURE DROP
                                                    0 kV/cm
                                                       36.0 mm
                                                    4 kV/cm
                                                       • 29.5 mm
                                                    2 kV/cm
                                                        26.8mm
                                                    6 kV/cm
                                                    APj « 13.0 mm
                  4           8         12
                   HOLE POSITION ACROSS FILTER
15
Figure  2.   Scan of permeability (expressed as pressure  drop at
  constant  air flow) for  dust cakes deposited at 0,  2,  4,
  and 6  kV/cm.  APC values  are for the  entire patch.

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B.  MEASUREMENTS OF CAKE DEPTH

       It was seen in the previous section that observed reductions
in pressure drop cannot  be accounted for by nonuniform dust
distribution across the filter face.  This implies that the amount
of dust per unit area of filter surface is likely to be fairly
uniform and that the patterns seen are due to differences in the
depth of penetration of the dust into the fabric.  To verify this,
four sets of layered filters were made.  Each set consisted of four
thin separable nonwovens  made by pressing a card web in a press for
a given time and at a given pressure.  The webs contained 15% of
a binde.r fiber  (vinyon) .  Copper wires, 150 ym in diameter, were
threaded into the upstream layers of each set in the usual configu-
ration (parallel wires, 15 mm apart/ alternate wires grounded),
and the sets used to filter a flyash aerosol.  Only one 5-minute
cycle was run, and each set was run at a different voltage.  After
a run the layers were separated and weighed.  The total mass of
dust collected on an absolute filter downstream of the main filter
was also weighed.  The fractions of dust captured by each layer and
the efficiency of each layer are plotted in Figures 3 and 4.  Only
one set of these measurements was performed, so that each point in
Figures 3 and 4 was obtained from only one measurement.  However,
the consistency of the  trends  within each curve and between curves
was taken as sufficient to make duplicate measurements unnecessary.

       When a field is applied, a major shift upstream occurs in
the dust deposition.  The fraction captured by the upstream layer
(layer number 1) increases from about 50 to nearly 90%, while that
captured on the three downstream layers decreases.  As the field is
increased to 4 and to 6 kV/cm,  the fraction collected on the down-
stream layers increases with a slight decrease in the upstream
layer that is not apparent in the log plot.  The total penetration
(given in Fig. 3) decreases considerably as field strength increases,
with a sharp decline between 4 and 6 kV/cm.  The calculated effi-
ciencies for each layer, plotted in Figure 4, show a sharp increase
for the two downstream layers at 6 kV/cm.

       When the layers were separated after filtering, it was
found that the penetration into the downstream layers was not
uniform.   Areas under the electrodes showed evidence of much greater
penetration (Figs. 5 and 6).  The deposits under the electrodes
were visually more pronounced as field strength increased.  This
greater deposition below the wires is assumed to account for the
measurements of greater fractional deposition on downstream layers
with increasing field strength.  The electrodes were 150-ym copper
wires so that onset of corona discharge should have occurred below
the lowest field used, i.e., 2 kV/cm.  The possible relationship
between these patterns of deposition and corona discharge will be
discussed in a later section.

       The above results appear paradoxical, since they mean that
in the presence of an electric field the dust accumulation in a
fabric is shifted in an upstream direction.  The greater mass

                              8

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     FRACTION
     COLLECTED
     ON LAYER
      1.0
      O.I
     0.01
    0.001
                                                            CAPTURE EFFICIENCY
                                                         ,or   OF LAYER
                                                         0.9 -
              I     2     3
              LAYER NUMBER
Figure 3.   Fractional collection on layers  of
  electrified layered filters,   o - 0 kV/cm,
  A - 2 kV/cm,  • - 4 kV/cm,  0-6 kV/cm.
                                                         O.I -
                                                                  LAYER NUMBEP
                                    Figure 4.   Capture efficiency of each layer of
                                      filters  in Figure 3.  o  - 0 kV/cm, A -  2  kV/cm,
                                      • - 4 kV/cm,  Q-6 kV/cm.

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                                LAYER 1
                                LAYER 2
                               LAYER 3
                               LAYER
Figure 5.  Upstream surfaces of layers of nonwoven fabrics
  of Figure 3 used to filter flyash at 0  (left) and 2  (right) kV/cm.
                                10

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                                LAYER 1
                                LAYER 2
                                LAYER 3
                                LAYER
Figure 6.  Upstream surfaces of layers of nonwoven fabrics
  of Figure 3 used to filter flyash at 4 (left) and 6 (right) kV/cm.
                                11

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 concentrated  in  the  first  layer would be  expected  to  lead  to
 greater  pressure drop.   In fact,  the  opposite  occurs/ and  we must
 conclude that cake formation  in the uppermost  layer must also  be
 modified by the  presence of the field.  The mass per  unit  area of
 layer  number  1 was about 62 g/m2.  Assuming a  fiber volume fraction
 of  0.1 and a  polyester density of  1.38, the thickness of the top
 layers was 0.45  mm.  The average  fiber-to-fiber distance s is
 given  by s =  (2ita2/a)%,  where a =  fiber radius and a  = volume
 fraction.  For the 3-denier fibers in these felts, s  was 55 ym
 and the  thickness of the upstream  layer was thus equivalent to
 about  eight layers of fibers.  It  was felt that the resolution
 of  the method was not sufficient to examine in greater detail  the
 events occurring in such small depths of  fabric.   Therefore, a
 different method was tried as described in the following section.


 C.  NEW  EMBEDDING PROCEDURE FOR CAKE'  CROSS-SECTIONING

       It has been reported previously [4] that microscopical
 examination of dust-cake formation by  scanning electron microscopy
 CSEM)  is not  informative,  for the  reasons that only the cake
 surface  can be examined and that the  electron  beam appears  to  disturb
 the cake structure by removing particles.  To  avoid these  diffi-
 culties, various  embedding and sectioning techniques were  tried.
 After  some unsuccessful attempts,  a procedure was  found that appears
 promising.

       A problem associated with flooding a fabric filter  bearing
 a dust cake with embedding fluid is the disturbance of the  cake by
 the fluid.  In some cases the dust cake can actually be caused to
 float off the fabric.  The new procedure consists  simply of extremely
 gradual  addition of embedding fluid to the dish in which the fabric
 sample lies,  so that the fluid seeps upward towards the cake by
 capillary action.  A small piece (about 1 square inch) of  the
 fabric with the dust cake on  it is carefully cut from a patch  and
 laid in  the bottom of an aluminum dish, cake side up.  The  embedding
 fluid is added to the bottom of the dish, a few millimeters from
 the edge of the fabric,  a drop about  every 15  s.  Addition  of  fluid
 is stopped when the sample gives the appearance of being only  wetted,
 rather than submerged.   Figure 7 shows, however, that even  at  this
 stage fabric interstices are  filled thoroughly.  The embedding fluid
was "Epon 812," manufactured by the Shell Chemical Co.

       Figure 7 is a composite optical photomicrograph of  a section
 through a commercial needled PET sample embedded in this fashion.
The section exposes a view into the thickness of the  fabric.  -The
dust cake is the dense area at the top of the photograph,  and  th6
air flow would be from the top downwards.  It  is interesting to
note that dust tends to lodge on the upstream  side of fibers,  sup-
 porting the assumption that the dust was not displaced by  the  medium.
 The photo also gives a simple illustration of  the  interaction  of
 fabric and dust.   At the upstream  surface the  heavy dust accumula-
 tion clearly presents few paths for dust penetration.  Further

                              12

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                      mm
                      . p

                                                              4*W



Figure 7.  Photomicrograph of cross section

  through commercial needled PET filter

  fabric and dust cake.

-------
 downstream dust can pass freely between  fibers  and  is  only  cap-
 tured when it impacts on one-   Particles are seen throughout  the
 filter,  but their number gradually decreases as depth  into  the filter
 increases.  The importance of  cake formation,  permeability,  and
 stability is somewhat better  understood  after examination of  the
 photo.


 D.   PHOTOGRAPHIC ANALYSIS OF  DUST CAKES

       The  method described in  the previous  section was now used
 to  determine the special features of the cake structure formed in
 the presence of an electric field that would account for the  lower
 pressure  drop usually found.  Two identical  patches of commercial
 needled PET fabric were  used.   One was fitted with electrodes.
 Both were used to filter a 5-g/m3  flyash aerosol at a face  velocity
 of  6 cm/s (12 ft/min)  with a  9-kV potential  applied to the  elec-
 trodes in the one patch.   The pressure drop  rose from 2 to  18 mm
 HaO without a field.   With the  field it  rose  to 3 mm.  This strong
 effect is frequently  obtained with clean  fabrics (i.e., fabrics
 that have not been "conditioned"  by repeated  filtering and  cleaning).
 Afterwards,  small pieces of fabric  were  cut  from each patch and
 embedded  as described above.  Micrographs of  cross sections from
 each sample are shown in Figure  8.  The detail of the cake  structure
 is  disappointing  since,  in both  cases, the cake appears as  a
 compact structure.  There  is no  obvious difference between  the two
 cakes and nothing that can be identified with lower pressure drop
 due  to ESFF.

       In a  different  approach,  the cakes were photographed with a
 camera fitted with a close-up lens.  Photos obtained in this fashion
 are  shown in Figure 9.   Here substantial differences can be seen at
 once.  In the absence  of an external field, the dust deposits in a
 smooth compact  cake.   Fibers protruding from  the fabric surface are
 free of dust.  With the  field applied, a great deal of deposition
occurs on these protruding fibers, and the entire appearance of the
cake is changed.

       The contrast between Figures 8 and 9 suggests that the
embedding procedure is not suitable for examination of the up-
 stream boundary of the dust cake.  The differences between Figures
 9a and 9b are not  apparent in Figures 8a and  8b.


E.  EFFECT OF FABRIC STRUCTURE

       Measurements of the change in performance obtained by
electrical stimulation of various fabrics indicate a strong depen-
dence of the effect on fabric structure.   Table I gives results
obtained with woven and nonwoven  (felted) fabrics made of glass
and polyester fibers.  It can be seen that on application of an
electric field, a  reduction in pressure drop is obtained only with
the nonwoven felts.  The three woven fabrics  (made  of untextured

                                14

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v f
                 •

                                             '•



            Figure 8.   Cross section through dust-coated fabric prepared
              by embedding procedure,
              a)  .Dust collected with no field applied.
              b)  Dust collected with 6-kV/cm field.  Peak on surface
                  occurs over electrode.

-------
Figure 9.  Photographs of the surfaces of the dust-laden filters
  in Figure 8.
  d) Dust collected with no field applied.
  b) Dust collected with 6-kV/cm field.

                              16

-------
          TABLE' I.  EFFICIENCIES AND PRESSURE DROP CHANGES DUE TO- ELECTRIC FIELD OF
                2 kV/cm APPLIED TO WOVEN AND NONWOVEN GLASS: AND' PET FABRICS
Producer
Style No.
Type
Material
wt. Cg/m2)
Wt. (oz/yd2)
AP (f ield)/AP (no field)
Burlington
486/38
Woven (2x2
Twill)
Glass
519
15.3
41/42
Cri swell
445-57/-DC2T
Woven (3x1
Twill)
Glass-
36£
10. -8
92/83
Owens-
Corning*
Non woven
Glass
473
12.9
28/49
Milliken*
—
Woven Fila.
(2x1 Twill)
PET
231
&. 8
53/55
Carborundum
918-404 9-45S~3'-0517
Nonwoven
PET
546
16. ±
25/>47/
  (AP in ram of water)

%E(field)/%EXno field)   70u. 2/57.0    86.7/&9..6
95.7/99.2
  Experimental- fabric

-------
yarn) give no reduction.  On the other hand, it is interesting to
note that all fabrics show increased capture efficiencies when the
electric field is applied.  It is conceivable, therefore, that the
mechanisms whereby penetration and pressure drop are reduced are
not the same.

       Further evidence of the importance of fabric structure to
the response to electrostatic stimulation is given by results of
an experiment in which a flyash aerosol was filtered through a
glass fabric  iided by the application of an electric field of
average strength 6 kV/cm.  The glass fabric was woven from a
combination of textured and untextured yarn.   (Texturing means
treating a yarn to impart a kind of permanent wave to each component
filament.  In an untextured yarn the filaments are straight and
closely packed.  Texturing separates the filaments and increases
the effective volume of the yarn by increasing the void volume
between filaments.)  The weave was such that one face of the fabric
was entirely covered with textured yarn.  This was the face designed
by the manufacturer to be exposed to the incoming dirty gas.  The
other face was roughly half covered by untextured yarn.  Two samples
of this fabric were fitted with electrodes, in one attached to the
textured face, in the other to the face having some untextured yarns
exposed.  Tne electrodes were coupled to a power supply as shown in
Figure Ic.   Figure 10 shows pressure drop ratios tPDR) obtained with
the two arrangements.  With no field applied, the pressure
drop was virtually equal at 36 mm H20 with either face upstream.
When an average field of 6 kV/cm was applied, however, the pressure
drop was  reduced 67% to 12 mm H20 with the textured face upstream,
but only 40% to 22 mm H20 with the partially untextured face
upstream.

       From these facts, the hypothesis can be proposed that in
order to increase pressure drop reductions, the fabric must have an
upstream layer of low fiber volume fraction.  The electric field
causes the cake to form preferentially in this low density region
by capture on single fibers,  rather than further downstream in the
denser portion of the fabric where the cake forms by bridging.
Where the low density region is absent, as in untextured filament
fabrics, no such changes in cake structure can be induced by the
field,  and there are practically no changes in pressure drop.

       The manner in which accumulation of dust in the low density
surface region may accomplish pressure drop reduction may be gauged
from the photo in Figure 9b and from Figure 11, which is a cross
section of the fabric shown in Figure 9 but with no dust.  The dust
in Figure 9b forms heavy encrustations on the surface fibers visible
in Figure 9a.  These encrustations look like cylinders with
diameters that range from 0.25 to 0.5 mm.  The broken-line circle
in Figure 11 represents the cross section of one such 0.25-mm
cylinder to scale, as if it had formed on the protruding fiber
visible at the top of the photograph.  This procedure is a construc-
tion of the kind of cross section that would have been obtained in

                                 18

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  PRESSURE DROP
     RATIO
  i.O r
  0.8 -
  0.6 -
                                           Fine yarn* on fac*

  0.41-
                                           Bulky yarn* on fact
                                         (Normal filtering surface)
          10    2030    40506070    80    90   OO
                          CYCLE NUMBER
Figure  10.  Effect of  fabric upstream  surface  structure  on
  pressure drop ratio.   Woven  glass bag.   Applied field:
  6 kV/cm.
                               19

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                                        v





                               v,t,t,  "•
                                            .
                                          3 '
                                        "'




                  *

                                               I

                        G    «-    ° C
                                o  .
Figure 11.  Cross section through the fabric used  for Figure  9
  but with no dust.  Broken circle indicates diameter of dust
  encrustation on surface fiber as in Figure 9b.   Horizontal
  band indicates equivalent thickness of dust layer.

-------
Figure 8a if the cross-sectioning technique had been successful.
Isolated fibers that protrude above the fabric appear to have a
remarkable ability to collect dust in an electric field.  The dust
cake photographed in Figure 9b had an areal density of 9xlO~3g/cm2.
The bulk density of the dust was approximately 1, so this mass is
equivalent to a layer 90 um thick.  This is also drawn in Figure 11
as a horizontal band.  It is interesting to note that if a parallel
array of cylindrical accumulations 0.25 mm in diameter spaced 0.4
mm apart were formed on the surface, all of the deposited dust
would be located in these cylinders.  Inspection of Figure 9b shows
that structures of this type occur with almost this frequency.
The pressure drop increase due to the cake formed in Figure 9a was
18 mm of water; that due to the cake in Figure 9b was only 1 mm of
water.  These observations provide a clearer picture of the changes
in dust cake structure that account for the reduction in pressure
drop with ESFF.  Previous accounts of these changes have offered
only qualitative observations such as that in the presence of a
field the cake was "more porous".

F.  STUDIES OF DENDRITE FORMATION

      A separate approach to explain the mechanism of pressure
drop reduction by ESFF was the study of the microstructure of dust
cake formations.  By this is meant the structure of the dust
collection at the single fiber level, as opposed to the structure
of the cake as revealed, for example, by the weighing of  filter
layers described in a previous section.  It appeared possible  that
the observed effect on pressure  drop might be a result  of changes
in the dust cake microstructure  as well as in the macrostructure.

      Basic structural configurations for the flyash deposits may
be postulated.  Two extreme cases are shown in Figure 12.  In  case
 Ca) all the particles stack on top of each other,  forming a  den-
drite at a specific location on  the fiber.  The  opposing possibil-
ity is illustrated by diagram  (b), where the particles  coat  the
fiber surface uniformly before they build the next  layer of  the
filter cake.  Theoretically these two cases ought  to give markedly
different filtration performance.  Butra J5J quite  reasonably  sug-
gests that a flyash deposit like (a) will collect particles much
more efficiently than the uniform coat  (b).   It  is  interesting to
note that the  flyash used at TRI has a particle  size distribution
such that the  submicron particles, because of their sheer numbers
 C\>105/cm3) / could build more extensive dendrites than the larger^
particles.  If  the cake develops by  surface coating, however,  then
the small particles become  less  dominant in the  collection process,
but may still  be important  if  they  act as  a glue and enhance
adhesion between larger particles.

      As for the pressure drop,  structure  (b}  should have less drag,
and consequently, a  filter  whose fibers become  coated uniformly  with
particles should have a  lower  pressure drop  than one whose fibers
 sprout dendritic growths.   This  argument applies to collection of
particles on fibers  Cinitial  filtration  stage)  or  to the capture of

                                 21

-------
               Dendrite Height ~ nr
                     (0)
                   Coating Height x nr~
                     (b)
Figure 12.  Basic  structural configurations  Figure  13.   Collection of charged particl*
  for flyash deposits  (schematic).              (a) charged and (b) neutral surfaces
                                                (schematic).
              Figure 14.  Micrographs of  flyash collected on trilobal poly-
                ester fibers  (a) with no  applied electric field and  (b)
                with a 4.2-kV/cm field.
                                             22

-------
pa.rti.cles by particles previously collected by fibers (later
filtration stages).  Of course these structures represent extremes
and the actual structures are most likely combinations of the two.

       It may be asked next,  what conditions favor the growth of one
structure over the other?  Since the high collection efficiencies we
have observed strongly suggest that the particles have some electric
charge, it is logical to consider the collection of charged particles
on charged and neutral surfaces.  Figure 13 illustrates these
situations.  The small solid circles represent particle positions,
the small dashed circles represent possible future positions of the
particles, the dotted lines denote particle trajectories, and the
large circles stand for fibers or larger flyash particles.  In case
(a) the collector is charged-either naturally, or by applying an
external field,-and t^e particles are more strongly attracted or
repelled by the collector surface than by each other, hence producing
a uniform coat.  In case (b), however, the collector is' neutral, and
the particle-particle electrical interaction dominates, giving a
dendritic growth.  Hence, the application of an electric field is
expected to yield a Ibwer pressure drop, since the cake microstructure
will be more compact  (ignoring, for the moment, macroscopic distri-
bution effects).  However,  it does not follow from this analysis
that the field should give a poorer efficiency.  Even though the
field will suppress dendrite growth, it also adds a force which
drives additional particles to the collector, the net effect being
to increase collection.

       In order to verify these postulates, the structure of cakes
deposited on individual fibers arranged in a regular, parallel array
in the presence or absence of a field was investigated microscopi-
cally.  The arrays were made of 120-ym fibers spread roughly 3 fiber
diameters apart, the average interfiber distance in a nonwoven fabric
filter.  They were exposed to the flyash for 330 s and observed from
the near stagnation point.   From the results, shown in Figure .14, it
is clear that the cake produced in the absence of an electric field
is more dendritic and fluffy than the deposit formed with a field.
Once more, the field does not entirely eliminate dendrites, but
serves to stunt their growth.  This should produce a lower drag and
may be a factor in the reduction in pressure drop with ESFF.


G.  EFFECT OF  CORONA

       It  is often  observed that the wire electrodes used to produce
the electric  field are bare,  and the  regions  of  fabric  immediately
surrounding the wires are clean on  the  side of the  filter facing
the flow, while dark  bands mark the positions of the  wires on  the
otherwise clean downstream face.   In  the experiments  using layered
filters,  these effects were  photographed  (Figs.  5 and 6).  It
appears,  therefore, that the particles  in  the region of the  wires
are more  difficult to capture and  penetrate farther into the filter.
This  effect  suggests  that  the aerosol is charged in the vicinity
of the wires,  probably  by  an ion cloud  surrounding the wire.

                                  23

-------
       The field  in a vacuum at the surface of two parallel  cylin-
drical conductors of diameter D whose centers are placed  a distance
S apart and maintained at a potential difference V is:
              E
                            V KS/D)2-!]
                surface   (S-D)  In {(S/D) +
The variation of  surface field calculated from this equation  with
voltage for different  size wires separated by 15 mm  (the  separation
most often used in our experiments)  is shown in Figure 15.  It
should be emphasized that this derivation neglects the effect of
fibers and particles on the field and should be used with caution
when applied to electrodes in a patch.  When the surface  field is
approximately 30  kV/cm,  corona, or the ionization of air  in the
vicinity of the wire,  occurs.  The convective velocity of the ions
due to the bulk flow is of the order of 10"1 m/s, but the field-
induced velocity  is roughly 10** m/s, and so the ions travel instantly
towards the opposite electrode.  Although the ion cloud may not
reach the other electrode due to interference from the fibers and
cake and collisions with air molecules, it does charge the fibers
and aerosol near  the wire to the same sign, and the two repel each
other, resulting  in no collection and clean fabric regions.
                  FIELD AT SURFACE
                   OF WIRE (kV)
                    IO
                          2    4    6   B   10
                            APPLIED VOLTAGE (kV)
12
          Figure 15. Variation of calculated surface field with applied
           voltage for wires of different diameters.


                                  24

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       After passing through, the region of like-charged fibers, the
aerosol is caught.  However, once the particles form a layer or two
on the fibers, the collection decreases since particles passing near
the now coated and hence charged fibers will be repelled as they
were from the clean charged fibers near the electrodes.  The parti-
cles must then pass to fibers deeper in the bed to be captured,
resulting in deeper penetration under the wires.
                                 25

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                            SECTION  IV

                    EFFECTS  OF  FIBER GEOMETRY


A.  MECHANISM  OF  PRESSURE DROP REDUCTION WITH  TRILOBAL FIBER  FILTERS

        In  the  previous  report  [4],  it was  concluded  likely  that
trilobal fibers enhance capture,  not only  because of reduced  inter-
 jiber distance, but also by the presence of localized electric
fields.  Calculations indicated that in the presence of electric
fields, lobed  fibers result in greater collection efficiencies than
round fibers.  If the aerosol  contains charged particles, their
deposition will set up  localized  electric  fields near the upstream
fabric  surface.   In the presence  of these  fields, capture of
subsequent particles will be more efficient on lobed fibers.
Further studies have yielded data consistent with this theory, and
have indicated how  this mechanism may also be  responsible for the
..oduced pressure drop obtained with trilobal fiber filters.

       The layered  filter technique was used  (see p. 7) to  measure
penetration and single  fiber efficiency for new trilobal and  round
fiber filters.  Now, similar data have been obtained with conditioned
filters.   Measurements  of flyash  retained before cleaning have been
made at the first,  twentieth,  and fortieth cycles, and plotted in
Figure 16.  It can  be seen  that at  the first cycle upstream layers
j'n the trilobal filter  collect slightly more than those in  the round
fabrics.   However,  as conditioning  progresses  a reversal takes place,
and the round fabric is  seen to retain more dust in  all layers.
This is equivalent  to saying that the dust is  cleaned more  easily
from the trilobal fabric, probably  because the dust  cake is formed
closer to  the upstream  surface in this fabric.  This lower  dust
retention  is accompanied by  a  lower  pressure drop.   There is  thus a
plausible  connection between lower  penetration and lower pressure
drop when  trilobal  fibers are  used  instead of round.


B.  X AND  Y-SHAPED FIBERS

       Progress in the  study of effects of fiber cross-sectional
shape on filtration performance is  limited in part by the lack of
appropriate fiber samples.    Thus,  in  studies of the  effects of the
number of  lobes in the cross section, the validity of the results
has,  in the past,  been diminished because no tetralobal fibers were
available,  and the pentalobal  fibers used had very shallow  lobes.
Moreover,  no series of  fibers with a range of lobe depths has to
date been  available.  Samples of  fibers with cross-sectional  shapes
different  from those used previously have now been obtained.  These
include nominal X, Y, and I  shapes, with linear densities of  3,5,
and 8 denier.   The fibers were  of crimped acetate supplied  by the
Celanese Fibers Company.
                                26

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                FLYASH RETAINED

               BEFORE CLEANING (q)
                                           All Loyers
                                             Remaining
                                              Layers
                        10    2O    30
                              CYCLES
40
Figure  16.  Flyash retained by  layered filters as  conditioning
  proceeds.
                                 27

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       Cross sections of these fibers are shown in Figures 17 and
18.  Figures 17b, c, and d are the 3-, 5-, and 8-denier Y fibers.
These have deeper lobes than the PET trilobal fiber used hitherto
whose cross section is shown for comparison in Figure 17a.  The
cross-sectional shape of a fiber can be described by an equation in
polar coordinates for a curve of the same shape.  In the equation


            p = . 1 + e cos m  ,


p is the radius vector, m the number of lobes, <|> the vectorial angle,
and e is a measure of lobe depth.  The diagram below shows an
example.  When e = 0, the cross section is circular.  Whereas the
trilobal PET fibers had an e value of about 0.25, the Y-shaped
acetate fibers have e values of about 0.6.  Figure 18 shows cross
sections of I and X fibers.  These shapes are generally more
irregular than the Y, and e values are more difficult to calculate.
       Nonwoven felt patches were made from each of these fibers,
and the fabric properties are listed in Table 2.  The performance
of each felt was measured on the patch apparatus using a flyash
aerosol with a concentration of 3.3g/m3.  The aerosol was neither
precharged nor neutralized, and no electrodes were placed in the
fabrics.  Measurements of pressure drop and penetration were made
after 20 conditioning cycles.  These are plotted in Figures 19 and
20.  It is interesting to note that felts made with these deep-lobe
fibers have better performance than those made with the PET trilobal
fibers.  Thus, in Figure 19 the pressure drop for Y fibers is

                                28

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Figure 17.  SEM cross sections of trilobal fibers:  a)  3-den
  PET, shallow lobe;  b) 3-den Y, acetate;  c) 5-den Y,
  acetate;  d) 8-den Y, acetate.

-------
                                                     .

Figure 18.   SEM cross sections of acetate fibers:
  b)  5-den X;   c)  8-den I.
                               30
a)  3-den I;

-------
significantly lower than that for the PET trilobal.   In Figure 20
the penetration is lower for the Y fibers than for the PET tri-
lobal.  The position in this performance scale taken by the X and I
fibers is less clear since,  while they produce higher pressure drops,
they also give lower penetrations.  It is not known how much the
differences are due to the different chemical compositions of the
fibers.  However, cellulosic fibers should have a higher electrical
conductivity.  This tends to dissipate electric charges and to lead
to poorer performance.  The differences seen in Figures 19-21 are
therefore unlikely to be due to the different compositions of the
fibers.


     TABLE 2.  PROPERTIES OF FELTS MADE FROM ACETATE FIBERS
                  WITH VARIOUS CROSS SECTIONS
Fiber
cross-sectional
shape
I
Y
X
Y
I
Y
Trilobal (PET)
Round (PET)
Fiber
linear density
(den)
2.62
2.67
6.03
5.31
8.24
8.35
3
3
Fabric
weight
(kg/m2)
0.257
0.255
0.256
0.258
0.257
0.256
0.251
0.253
Fabric
density
(g/cm3 )
0.142
0.134
0.150
0.151
0.146
0.147
0.134
0.138
       So-called "performance curves" have been plotted in the past
16] to allow for the trade-off between pressure drop and penetration
as fiber linear density changes.  These curves are developed by
plotting penetration vs. pressure drop  (or some equivalent parameter),
as in Figure 21, and ideal performance is represented by a point at
the origin.  Performance points for felts made of fibers with a
particular cross-sectional shape but of different linear densities
will fall on a characteristic curve.  The distance of the curves from
the origin can be taken as a measure of the performance associated
with that fiber.  This criterion applied to the results in Figure
21 shows that, in fact, the Y fibers produce a curve which is closer
to the origin than the PET trilobal fibers.  The points in Figure 21
represent an incomplete collection, which will be filled in the
future.  In addition, the performance curves show,that the Y fibers
make for slightly better performance than the I fibers.  From the
cross sections shown in Figure 18 it would appear that the X fibers
should give performance very similar to that of I fibers since they
all approximate irregular tetralobal shapes.  The results in Figure
21, however, show that the X fibers are slightly better, though it
is impossible to identify a feature of their cross section to which
this better performance may be attributed.

                                 31

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                                                  PENETRATION
                                                   .004
    IOO


    9O


    80


    70


    60


    50
A—TRILOBAL PET
0«-ROUND PET
                                     .003
             ACETATE
              I-SHAPED
               Y-SHAPED
                 X-SHAPED
.002-
                      i - 8-
                   10
             LINEAR DENSITY (dm)
                                                   jOOl
Figure  19.   Comparison of pressure  drop with
  fabrics made of I,  Y,  and X-shaped acetate,
  trilobal  PET (A),  and round PET (o)  fibers.
                                                                  -ROUND PET
                                                A—TRILOBAL
                                                    PET
                                                                     ACETATE

                                                                     Y-SHAPED

                                                                     I-SHAPED
                                                                                  X-SHAPED
                                                             LINEAR DENSITY (dm)
                                                                                	
                                                                                 10
                                        Figure  20.  Comparison of penetration  (1 -  effi-
                                          ciency)  with fabrics made of  I,  Y, and X-
                                          shaped acetate,  trilobal PET  (A), and round
                                          PET  (o)  fibers.
                                          TRILOBAL\
                                                  \
                                             ACETATE
                                             I-SHAPED
                                             Y-SHAPED
                                             X-SHAPED
                                                       ROUND PET
                             20-
                                   .OOI
                           .002   003
                            PENETRATION
                                                         .005
                    Figure 21.  Performance curves for the  fabrics
                       in  Figures 19  and 20.
                                           32

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       A previous report [4]  gave results of calculations of single
fiber efficiencies in electric fields for fibers with different
lobe depths.  The results indicated a strong direct dependence of
capture efficiency on lobe depth. . These results have suggested the
possibility that the better performance of lobed-fiber filters may
be due to the better capture behavior of these fibers in localized
electric fields due to deposited charged aerosol particles.  No
experimental verification of the hypothesis has been made, but the
better performance with deep-lobed fibers reported above appears
to support it.


C.  COMPOSITE FILTERS

1.  Initial Cycles

       The last report [4]  described measurements on filters made
by pressing together layers of vinyon-bonded nonwovens made with
different fibers.  The fibers used at that time were 3-denier
trilobal and 3-denier round cross section polyester.  It was found
that the upstream layers appeared to control the behavior of the
filter.

       Measurements of this type were repeated with layers differing
in fiber fineness, namely with 3 and 6-denier trilobal polyester.
Table 3 describes the combinations used; just as in the first study,
two filters had all layers composed of either 3 or 6-denier fibers,
the other two had a top layer of one fiber and the remaining 5
layers of the other.  Trial conditions were identical with the first
study.  At the twentieth cycle of conditioning, the trials were
terminated and measurements recorded.


       TABLE 3.  COMPOSITE FILTERS MADE OF 3 AND 6-DENIER
                    TRILOBAL POLYESTER FIBERS
                    Upstream      Downstream
                     layer	      layer	

                       All 6 denier
                       (0.25 kg/m2)

                       All 3 denier
                       (0.25 kg/m2)

                  6 denier       3 denier
                  (0.04 kg/m2)   (0.21 kg/m2)

                  3 denier       6 denier
                  (0.04 kg/m2)   (0.21 kg/m2)
                               33

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       Figure 22 shows an unexpected trend in pressure drop behavior
for the four fabrics during conditioning.  In the first 10 cycles,
the upstream layers dominate the behavior, just as in the study of
cross-sectional shape.  Thereafter, a reversal in the trend appears,
with pressure drop now being determined by the downstream fibers.
A similar crossover occurs in the pressure drop rise within one
cycle  (the 20th) shown in Figure 23.

       These phenomena are assumed to be the result of dust seepage
past the upstream layer, so that as the dust deposit advances,
responses characteristic of the downstream layers appear.  Since
these data showed evidence that behavior had not yet stabilized, it
was difficult to make any additional conclusions concerning fine/
coarse composites.  A new trial was initiated.

2.  Conditioned Fabrics

       A second study of fine/coarse composites was carried out
using the following series of samples:


                    Upstream   /   Downstream

                     0% 6d          100% 3d
                    17% 6d           83% 3d
                    50% 6d           50% 3d
                    83% 6d           17% 3d
                     0% 3d          100% 6d
                    17% 3d           83% 6d
                    50% 3d           50% 6d
                    83% 3d           17% 6d


The samples were vinyon-bonded at a higher temperature .than had
previously been used (I2l°c instead of 99°C), thereby achieving a
more stable fabric density.  Measurements were made after a longer
conditioning than reported previously (30 to 40 cycles instead of
20 cycles).  Each data point is the average of from 2 to 5 measure-
ments using replicate samples or vacuum-cleaned samples.  The above
steps were intended to further increase the reliability of the
results.  Experimental conditions were as follows:

       Fabric weight      :  0.25 kg/m2(7.3 oz/yd2)
       Fabric density     :  0.130 g/cm3
       Fiber type         :  PET
       Face velocity      :  60 mm/s (12 ft/min)
       Inlet concentration  :  3.5 g/m3
       Cycle time         :  5. min
       Pressure in reverse air cleaning  :  209 kPa (30 psi)

       Measurements were made not only of the penetration and the
pressure drop of these filters-, but also of the residual dust after
cleaning (expressed as a fraction of the base filter mass).  Figures
24, 25, and 26 show these measurements as a function of composition

                                34

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                                            .JQ All 3 Denier

                                              6 Denier,
                                               upstrean
                                             -A 3 Den upttrenra
                                             3 All 6 Denier
                   5        10        15
                        NO. OF CYCLES
20
Figure 22.   Changes  in pressure drop  during  conditioning of
   composite  PET filters.
        AP DURING 20 TH CYCLE
            (mm HgO)
                                          ALL 3 DENIER

                                         * 6 DEN UPSTREAM

                                          3 DEN UPSTREAM
                                          ALL 6 DENIER
                 I    234567
                   CAKE DEPOSITION (mg/cm2)
Figure 23.  Changes  in  pressure drop during the  20th cycle
  for  composite PET  filters.
                                35

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by weight  (% 6d/% 3d) of the two-layer composite filters.  In
these graphs, percentage of 6-denier fibers upstream increases to
the right, whereas percentage of 3-denier fibers upstream increases
to the left.  It can be seen now that a composite with 3-denier
fibers upstream allows less penetration and also exhibits a lower
pressure drop than one with 6-denier fibers upstream or one with
100% 3-denier fibers.  The 17% 3d upstream/83% 6d downstream
composite appears to be optimum.

     These effects may be explainable by the correlation between
the curves of Figures 24 and 25 with those of Figure 26.  It
appears generally that penetration and pressure drop are directly
related to the amount of dust retained after cleaning.  Finer
(3-denier) fibers upstream prevent dust from lodging deeper into
the filter where it cannot be blown back.  This in turn keeps the
penetration lower, and since unremovable dust increases resis-
tance, also keeps the pressure drop lower.  The slightly upward
turn of the pressure drop curve at 100% 6d may also be due to
increased residual dust.  Although 17% 3d/83% 6d appears to be
optimum, further studies with commercial-weight filters should
be conducted to verify these findings.
                                36

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       AP(mmH201
        120 H
                             PENETRATION (X)
                              0.8
          O/OO 17/83
50/90     83/17  100/0
X8d/X3d
0/WO 17/83      50/50     83/17 DO/0
            X6d/X3d
Figure 24.   Pressure drop across  composite  Figure  25.  Penetration through, the coitposite
  vinyon-bonded PET filters  having varying     filters of Figure  24.   Solid circles  are
  proportions  of 3 and 6-denier  fibers in      points for all  3 or  all 6-denier filters.
  two layers.
                            	(CLEANING
                             (Xofwt fabric)

                             300-
                              CMOO   17/83      50/50     83/17  100/0
                                          X6d/X3d
                         Figure 26.   Residual dust after cleaning
                           the filters  of Figure 24.
                                              37

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                            SECTION V


                            REFERENCES
1.   Endres, H.  A.., and W. T. van Orman, Electrostatic Properties
     of Rubber and Plastics, SPE Journal 26 (Feb. 1953).

2.   Silverman,  L. et al.f Performance of a Model K Electro-Polar
     Filter, USAEC Report NYO 1592, Harvard University, July 15,
     1954.

3.   Thomas, J.  W. and E. J. Woodfin, Electrified Fibrous Air
     Filters, AIEE Journal, 276-278  (Nov. 1959).

4.   Miller, B., G. Lamb, P. Costanza, D. O'Meara, and J. Dunbar,
     Studies of  Dust Cake Formation and Structure in Fabric Filtra-
     tion, EPA 600/7-78-095, June 1978.

5.   Butra, S.,  Aerosol Particle Deposition in Fibrous Media with
     Dendritic Pattern.  Comparison Between Theory and Experiment,
     Master's Thesis, Department of Chemical Engineering, University
     of Houston, March 1978.

6.   Miller, B., G. Lamb., P. Costanza, and J.  Craig, Nonwoven Fabric
     Filters for Particulate Removal in the Respirable Dust Range,
     EPA 600/7-77-115, October 1977.
                                 38

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                                TECHNICAL REPORT DATA
                         (Please read Instructions on the reverse before completing)
  REPORT NO.
 EPA-600/7-79-108
                                                      3. RECIPIENT'S ACCESSION NO.
 TITLE AND SUBTITLE
Studies of Dust Cake Formation and Structure in
 Fabric  Filtration: Second Year
                                                      5. REPORT DATE
                                                       April 1979
                                                      6. PERFORMING ORGANIZATION CODE
         Bernard Miller, George Lamb,Peter Cos-
tanza,George Harriott,Janet Dunbar,  and Michael
Mnkricki
                                                      8. PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AND ADDRESS
 Textile Research Institute
 P.O. Box 625
 Princeton, New Jersey  08540
                                                      10. PROGRAM ELEMENT NO.

                                                      EHE624A
                                                      11. CONTRACT/GRANT NO.
                                                      Grant R804926
12. SPONSORING AGENCY NAME AND ADDRESS
                                                       13. TYPE OF REPORT AND PERIOD COVERED
 EPA, Office of Research and Development
 Industrial Environmental Research Laboratory
 Research Triangle Park, NC 27711
                                                      13. TYPE OF REPORT
                                                      12/77 - 12/78
                                                      14. SPONSORING AGENCY CODE
                                                        EPA/600/13
^.SUPPLEMENTARY NOTES
                              pr0ject officer & James H. Turner, MD-61, 919/541-
 2925. Report EPA-600/7-78-095 covers the first year's work.
16. ABSTRACT
          The report describes experiments to improve fabric filter efficiency and
 pressure drop by use of electric fields near the filter surface. Modified fiber geo-
 metries and fabric construction are also investigated. Tests with patch filters
 showed pressure drops reduced to about 13 mm H2O from about 36 mm H2O upon
 the application of a 6 kV/cm electric field. Total fractional particle penetration was
 reduced to about 0.001 from 0.170 under the influence of the same field. The electric
 field was more effective when applied to filters having loose fibers  at the  surface.
 Deeply lobed fibers produced filters with higher efficiency, lower pressure drop,
 and better cleanability than filters made from round fibers. The effects were attri-
 buted to induced localized fields  at the lobed surfaces. The fields were produced
 from  collection of naturally charged particles.  Fabric structure that promotes par-
 ticle collection near the upstream surface of the filter gave the best performance.
17.
                             KEY WORDS AND DOCUMENT ANALYSIS
                 DESCRIPTORS
                                           b. IDENTIFIERS/OPEN ENDED TERMS
                                                                     COS AT I Field/Group
 Pollution
 Gas Filters
 Fabrics
 Dust
 Caking
 Electric Fields
                      Fibers
                      Shape
Pollution Control
Stationary Sources
Fabric Filters
Particulate
13B
13K
HE
11G
07A,13H
20C
12A
~8. DISTRIBUTION STATEMENT
 Unlimited
                                          19. SECURITY CLASS (This Report)
                                           Unclassified
                                                                    21. NO. OF PAGES
                                                                        45
                                          20. SECURITY CLASS (This page)
                                           Unclassified
                         22. PRICE
EPA Form 2220-1 (9-73)
                                         39

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