EPA-670/2-74-017
March 1974
Environmental Protection Technology Series
               VALUATION AND DEMONSTRATION
            OF  THE CAPILLARY  SUCTION SLUDGE
                              DEWATERING DEVICE
                                National Environmental Research Center
                                  Office of Research and Development
                                  U.S. Environmental Protection Agency
                                         Cincinnati, Ohio 45268

-------
                                     EPA-670/2-74-017
                                     March  1974
EVALUATION AND DEMONSTRATION OF THE CAPILLARY

      SUCTION SLUDGE DEWATERING DEVICE
                     By
                T. E. Lippert
                M. C. Skriba
      Westinghouse Electric Corporation
       Research and Development  Center
       Pittsburgh, Pennsylvania   15235
           Program Element  1B2043
               Project Officer

              J. E. Smith, Jr.
Advanced Waste Treatment Research  Laboratory
   National Environmental Research  Center
           Cincinnati, Ohio   45268
   NATIONAL ENVIRONMENTAL  RESEARCH  CENTER
     OFFICE OF RESEARCH AND  DEVELOPMENT
    U.S. ENVIRONMENTAL PROTECTION AGENCY
           CINCINNATI, OHIO   45268

-------
                          NOTICE

     The Rational Enviroxnental Research Center —
Cincinnati baa rerleved this report and approved
its publication.  Approval does not signify that
toe contents necessarily reflect the views and
policies of the U. 8. Environmental Protection
Agency, nor does mention of trade naaes or con-
nercial products constitute endorsement or recom-
nendation for use.
                        li

-------
                      FOREWORD
    Man and his environment must be protected from the
adverse effects of pesticides, radiation, noise and other
forms of pollution, and the unwise management of solid
waste.  Efforts to protect the environment require a
focus that recognizes the interplay between the com-
ponents of our physical environment—air, water, and
land.  The National Environmental Research Centers
provide this multidisciplinazy focus through programs
engaged in

      •   studies on the effects of environmental
          contaminants on man and the biosphere, and

      •   a search for ways to prevent contamin-
          ation and to recycle valuable resources.

    The research reported here was performed for the
Ultimate Disposal Section of the Advanced Waste Treatment
Research Laboratory to develop and demonstrate a new
method of activated sludge (concentrated pollutant stream)
dewaterlng.  Since sludge hMHUwg and disposal represents
a significant part of the total wastewater treatment cost,
a new dewatering technique which promises higher cake
solids at higher loading rates and a cleaner filtrate at
reduced cost is very welcome.
                                 A. W. Breidenbach, Ph.D.
                                 Director
                                 Rational Environmental
                                 Research Center, Cincinnati
                         in

-------
                               ABSTRACT
A device for dewaterlng waste activated sludge that uses the capillary
suction in a porous belt has been demonstrated on a pilot scale test
unit.  The system uses capillary action to initially dewater the sludge
and form a thin sludge cake which is then mechanically compressed in a
final step to obtain a still dryer cake.  Both dewatering steps are
incorporated into a single system endless belt design.  Sludge feed
capacities from 2 to 4.5 Ibs/hr ft2  (10 to 22 Kgs/hr m2) have been
demonstrated with the cake solids at discharge ranging from 15 to 18
percent.  These results were obtained with a conditioned waste activated
sludge at a coagulant cost of approximately $4.00/ton  ($4.40/metric ton).
The device has also been tested on an anaerobically digested and a
mixed primary-activated sludge.

This report was submitted in fulfillment of Research Contract 68-01-0094
under the sponsorship of the Environmental Protection Agency, Advanced
Waste Treatment Research Laboratory,
                                    iv

-------
                               CONTENTS

SECTION                                                           PAGE

  I        CONCLUSIONS AKD RECOMMENDATIONS   	  1

  II       INTRODUCTION  	  2

  III      EXPERIMENTAL APPARATUS  	  5

  IV       DISCUSSION OF RESULTS	21

  V        REFERENCES	55

  VI       APPENDIX A - Error Analysis	56

  VII      APPENDIX B - A Chronological Summary Listing of
                        Test Data - Pilot Test Unit	60

  VIII     APPENDIX C - Economics of Capillary Dewatering of
                        Waste Activated Sludge	66
                                     v

-------
                                FIGURES

No.                                                               Page

  1       Schematic of Research Capillary Dewatering Unit  ....    3

  2       Laboratory Capillary Dewatering Unit ....  	    6

  3       Capillary Dewatering Pilot Test Unit	    7

  4       Schematic of Demonstration Test Unit	    8

  5       Schematic of System Set-Up   	    9

  6       Westinghouse Test Facility at the Long Road Sewage
         Plant	   11

  7       Long Road Sewage Treatment Plant - Flow Schematic  ...   12

  8       Sludge Specific Resistance - Waste Activated Sludge  .  .   1^

  9       Sludge Specific Resistance - Mixed Activated Primary   .   15

10       Sludge Specific Resistance - Anaerobically Digested  .  .   16

11       Endless Belt Life Test Apparatus for Evaluating Porous
         Media Swatch Samples	   17

12       Porous Media Swatch Samples Before Entering Sewage   .  .   18

13       Sludge Capillary Dewatering Curves  	   24

14       Capillary Dewatering-Machine Capacity with Waste
         Activated Sludge  	   25

15       Capillary Dewatering - Comparison of Digested and Mixed
         Sludge Data with Design Curve for Waste Activated
         Sludge	   27

16       Capillary Dewatering - Calculated Machine Capacity  . .   28

17       Capillary Dewatering - Calculated Machine Capacity  . .   30

18       Capillary Dewatering - Calculated Machine Capacity  . .   31

19       Capillary Dewatering - Calculated Machine Capacity  . .   32

20       Correlation of Machine Apparent Capacity with Sludge
         Specific Resistance for Two Coagulant Types 	   33

-------
                                 FIGURES

No.

21       Schematic Arrangement of Swatch Test Apparatus for
         Simulating Capillary Dewatering  ..............   35

22       Belt Pore Size Effect on Capillary Dewatering Cake
         Solids ...........................   36

23       Porous Felt and Reinforcing Scrim  .............   37

24       Five Basic Porous Material Swatch Samples Before and
         After 30 Days Testing  ...................   38

25       Swatch Samples After 3 1/2 Months  .............   39

26       Swatch Samples After 12 Months   ..............   **0

27       Photograph of Porous Belt From Pilot Unit After 12
         Months of Testing  .....................   k2
28       Capillary Dewatering - Final Cake Solids   .........  W-

29       Effect of Coagulant Dosage on Final Cake Solids  ......  ^5

30       Photograph Depicting Sludge Cake Detachment  ........  47

31       Effect of Screen Mesh Size on Solids Capture   .......  k8

32       Capillary Dewatering - Sludge Cake Solids Capture  .....  ^9

33       Capillary Dewatering - Sludge Cake Solids Capture  .....  51

34       Capillary Dewatering - Sludge Cake Solids Capture  .....  52

35       Capillary Dewatering - Sludge Cake Solids Capture  .....  53
                                    vii

-------
                                 TABLES

No .                                                                 Page

1        Sludge Properties ....................    10

2        Sample Data Sheet   ...................    19

3        Expected Uncertainty in the Calculated Quantities ....    20

4        Summary of Pilot Plant Capillary Dewatering System
         Performance .......................    21
5        Porous Material Physical Properties

1-A      Expected Uncertainty in Measured Variables
1-B      Pilot Test Unit - Summary of Data From May 22 Through
         August 10, 1972 - System Installation and Shakedown   .  .   6l

2-B      Pilot Test Unit - Summary of Data From August 16
         Through October 4, 1972 - Base Line System Performance  .   62

3-B      Pilot Test Unit - Summary of Data from October 11
         Through November 16,  1972 - Initial Study of Machine
         Parameters on Waste Activated Sludge  ..........   63

4-B      Pilot Test Unit - Summary of Data From December 1
         Through January 1, 1972-73 - Continue Study of Machine
         Performance on Waste  Activated Sludge   .........   6*4-

5-B      Pilot Test Unit - Summary of Data From January 26
         Through February 14,  1973 - Continue Study of
         Machine Performance with Digested and Mixed Primary
         Sludges   ........................   65

1-C      Cost Estimate for Capillary Dewatering  .........   68
                                  vlli

-------
                               ACKNOWLEDGMENTS
This project was conducted at the Westinghouse Research and Development  Center
by Dr. T. E. Lippert,  and Mr. M.  C.  Skriba,  under the  management  of Mr.  R.  M.
Chamberlin, Manager of the Ecological Systems Department.

The support of the project by the Environmental Protection Agency and the many
useful contributions made by Dr.  J.  E. Smith, Jr., Project Officer, is greatly
appreciated.

The bulk of the experimental testing was conducted at  the  Westinghouse test
facility located at the Long Road Sewage Treatment Plant,  Penn Hills, Pittsburgh,
Pennsylvania, under the capable guidance of  Mr. R. F.  Watson.  The cooperation
of the sewage plant personnel, Mr. Ronald Young, Mr. Ernest O'Malley, and
Mr, Matthew Drop and the cooperation of the  Penn Hills Municipal  Authorities
is greatly acknowledged.

Sampling and analysis throughout the test program were performed  by Mr.  M.  J. Testa,
Mr. J. W. Parks, and Mr. C. G. Slater.  The  typing of the  manuscript was done by
Miss Darlene Kuszyk.
                                        iac

-------
                                SECTION I

                     CONCLUSIONS AND RECOMMENDATIONS

A device for dewatering waste activated sludge that uses the capillary
suction in a porous belt has been demonstrated on a pilot scale test
unit.  The device was also tested on an anaerobically digested and a
mixed primary/activated sludge.   Feed capacities from 2 to 4.5 Ibs d.s./
hr ft2 (10 to 22 Kgs/hr m2) were achieved with the cake solids at
discharge ranging from 15 to 18 percent for activated sludge.  Machine
capacities more than twice these values may be possible.  It was found
that the device can be operated without coagulant addition at a penalty
to solids capture.  With chemical addition of the polyelectrolyte at
10 Ibs/ton (5 Kgs/metric tons) or about $4.00/ton ($4.40/metric ton)
a cake solids capture of 95 percent can be obtained when the machine is
operated at 2.0 Ibs/hr ft2 (10 Kg/hr m2) .  Operating at higher machine
capacities, i.e., 4.0 Ibs/hr ft2 and higher, it appears that the ferric
chloride conditioner yields more economical system operation.  Overall
machine operation was found to depend on chemical addition, sludge solids
loading and screen mesh size.

This study has led to the development of a sound engineering understanding
of the operation of this device including the advancement and development
of specific design curves applicable to the particular waste activated
sludge used.  It is recommended that supporting data from other plants on
waste activated sludge be developed to verify these results.  Furthermore,
additional data and analysis is required to optimize system capacity
with respect to both solids loading and chemical addition.  Present data
Indicates that such an analysis could lead to developing machine capacities
as high as 20 Ibs/hr ft2 (100 Kg/hr m2).  Additional screen evaluations
are needed to establish if screen type and design significantly effect
the capillary dewatering rate and sludge cake detachment (i.e., prefer-
ential adherence to the compression roller as opposed to staying attached
to the screen).  Operation of a full scale field unit is required in
order to establish realistic operating and total cost figures.
                                 - 1 -

-------
                                SECTION II

                               INTRODUCTION
 Frequently a sludge must be dewatered before it can be satisfactorily
 disposed of, and the dewatering process is one of the most costly
 involved in the handling and disposal of sewage solids.  The quantities
 of sludges to be handled and the difficulties in handling and disposing
 of these sludges increase directly with the quality of the treated
 wastewater product.(1)  The Federal Water Pollution Control Act Amend-
 ments of 1972 provide for improved wastewater quality including secondary
 treatment or its equivalent for municipal discharges by 1977, (2)
 In most cases this will require treatment plants to include biological
 treatment although in some it may only mean upgrading existing processes
 with chemical addition.   Either alternative will cause more sludge to
 be produced,  and this sludge will probably be more difficult to process.

 Sludges which present a problem to mechanically dewater include waste
 activated and  chemical sludges.   This is partly because  of their
 diluteness and  partly because of  their gelatinous  nature.   Presently
 very few municipalities  will dewater only a waste  activated sludge,
 even after first thickening  it.   It is almost always  first  combined  with
 a  primary sludge,  even though it  is well  known that  the presence of  waste
 activated sludge increases  the  cost of dewatering  primary  sludge.
 Conventional  dewatering  equipment  is unable to  dewater straight  waste
 activated sludge unless  prohibitive quantities  of chemicals  are  added.

 The  Westinghouse Electric Corporation over  the  last  three years  has  been
 Involved in developing a unique method to dewater  dilute sludges.  This
 work  over the last  year  and  a half  has been supported  under  EPA  contract
 specifically  to  answer the need for an economical  mechanical  dewatering
 system  for use with unthickened waste activated  sludge.  Although  thickened
 activated  sludge and other sludge  types were also  evaluated,  the proposed
 system  should produce a  truckable  cake and/or a  cake capable  of  under-
 going combustion with minimum fuel  requirements.

 The system under development uses capillary action to  initially dewater
 the sludge and form a thin sludge cake and  it then employs mechanical
 compression to obtain a  still drier  cake.   Both these  dewatering steps
 are incorporated into a  single system, endless belt design.  A schematic
 of the device is shown in Figure 1.   The endless belt  portion of the device
 is actually comprised of two belts; a belt made of a porous material
 approximately 1/2 in.  (13 mm) thick and a fine mesh screen belt.

To operate this  device,  the sludge is generally preconditioned, and then
pumped onto the top at one end of the screen belt in a thin layer while
both the porous  and screen belts move towards the opposite end.  The
porous belt provides the capillary action for dewatering while the
screen belt carries the sludge and serves to minimize clogging of the
                                  - 2 -

-------
                               Sludge
                                Cake
                      Sludge
                   Compression
                       Roller
            Sludge Feed
Capillary Dewatering Section
                                                                                      Sludge
                                                                                      Cake
u>
I
                                           Belt & Screen Motion
                                                    mutt Hit Itmimiiiiill
                                        Screen
                                        Wash
                 Cake
                Filtrate         Porous
                                Belt
                    Screen
                     Belt
                       Fig. 1 -Schematic of research capillary dewatering unit

-------
 belt pores by the sludge solids.  The porous belt, screen belt, and
 sludge are in direct contact which allows the free water associated with
 the sludge to be drawn preferentially by capillary forces through the
 screen belt into the porous belt.  The sludge solids remain on the
 screen.  By the time the sludge has reaqhed the end of the capillary
 section of the machine, it has been transformed from its initial liquid
 form to a semi-solid thin sludge cake containing typically from 6 to 10
 percent solids by weight.  At this point, the sludge cake is passed
 under a compression roller causing additional water to be extracted.   It
 has been found that the final solids  of the cake depend on many factors
 but a 16 to 20 percent cake is typical for a waste activated sludge.
 This compression roller also serves as the sludge cake removal mechanism.
 The sludge cake after being compressed attaches  preferentially to the
 roller surface and is lifted away from the screen belt.   This  provides
 for an effective method of detaching  the  thin sludge cake and  thereby
 maintaining a  high solids recovery.   The  water that  was  extracted from
 the sludge is  contained within the porous belt and  is  subsequently
 squeezed-out and the  belt and screen  returned to  the feed position.

 The practice of  using  capillary  action for  solid  liquid  separation  is
 not new (3,4),  nor  is  the application  of  belt  and sludge  presses  to
 sludge dewatering.(5)   However,  the capillary  suction  device described
 above  is an improvement  over  prior  systems in  that it  incorporates both
 these  process operations  in an arrangement that allows effective  sludge
 dewatering  and  cake detachment with a minimum  of energy expended.  More-
 over,  the  results of this study provide an improved  technological basis
 of  the  design and performance of  this capillary suction device.

 The  scope of this program has included both an evaluation of the basic
 mechanical  functions of the device as  well as a determination
 of specific design relationships.  Machine performance on a pilot scale
 system was evaluated on three sludge types; the evaluation included
 first a determination of overall machine performance, such as system
 capacity and final cake solids, and secondly an evaluation of certain
design parameters such as screen mesh  size, capillary belt pore size,
and compression roller force.

-------
                               SECTION III

                         EXPERIMENTAL APPARATUS

CAPILLARY DEWATERING APPARATUS

Two experimental capillary dewatering test units have been operated.
The first unit, shown in Figure 2,  is a small scale system approximately
4 inches (10.1 cm) wide and 2 1/2 ft. (0.76 m) long (1 lit/min max.
sludge feed rate).  During the course of this program, this unit was  used
to generate the basic data for evaluating the mechanical operation of
the system and determining parametric interactions.  The second unit
(or pilot unit), shown in Figure 3, is about 1 ft.  (0.30 ra) wide and
5 ft. (1.5 m) long and has six times the capacity of the smaller unit.
This unit was built later and operated at a local sewage treatment plant
to determine overall system operation and to substantiate results obtained
from the smaller unit.

A schematic layout of the pilot test unit is given in Figure 4.  Originally,
this unit was designed so the porous belt and screen belt would track
over separate drive rollers.  This was later changed so that both the
porous belt and screen belt track over the aft drive roller.  The porous
belt is driven by a combination of the tension force exerted around the
aft roller and the drive force imparted to the belt by the set of
compression rollers indicated in the schematic.  This drive arrangement
allows a minimum tension force on the porous belt thereby eliminating
any belt stretch problems.  The set of belt compression rollers also
serve as the method of extracting the belt water (cake filtrate).  Three
water spray nozzles are located beneath the aft drive roller and are used
to wash the screen belt which, at this location, is separated from the
porous belt.  The cake filtrate and wash water streams are maintained and
sampled separately.  The porous and screen belts are driven from a 1/2 hp
(40 Kg-m/sec) variable speed motor using chain and sprocket drives.
Screen material used in the program was a dacron polyester supplied by
Wire Cloth Enterprises, Pittsburgh, Pa.  Porous belt material was a nylon,
needle punched felt of approximately 7 oz/ft2 density (2.2 Kg/m^)
supplied by Orr Felt Company, Piqua, Ohio.

The general arrangement of the test unit, sludge and chemical feed
pumps is given in Figure 5.  The sludge was drawn from the sewage plant
at the return line using a positive displacement 2.0 gal/min  (7.5 lit/min)
pump and a 2-inch  (52 mm) line.  Sludge for the dewatering unit was
drawn from this line via a smaller (0-6 lit/min) pulsation pump.  The
unused sludge was circulated back to the primary treatment tank.  This
arrangement provided fresh sludge continuously.  Coagulant was prepared
in stock solutions and pumped from a holding tank into the sludge line
on the output side of the pulsation pump.  There were approximately  3 ft.
(1 m) of 3/4 inch  (19.0 mm) tubing in which the sludge and coagulant
were mixed before spilling into the feed tray.  The feed tray utilized a
splitter plug to dampen flow variations, thus assuring a uniform sludge
layer onto the dewatering unit.
                                   -  5 -

-------
Fig. 2 - Laboratory capillary dewatering unit

-------
Fig. 3 - Capillary dewatering pilot test unit,
                    - 7 -

-------
 I
03
                                Belt And Screen
                                Adjustment    Feed
                                                Reservoir
Capillary
Dewatering
  Section
Sludge
Compression
Roller
Compression Rollers
(Alternate Position)
                                                           Scale 1cm ±.13 Meters
                                                 Fig. 4- Schematic of demonstration test unit

-------
SO
I
                Coagulant
                Feed Tank
               Sludge Bypass
               To Drain
                     Moyno
                  Sludge Pump
                        t
IL

 Feed
Pump
                                                Test Unit
                                          Cake Filtrate
                                          to Drain
                                      Sludge
                                       Feed
                                      Pump
               Screen Wash
               Water to Drains
                 Bypass to Drain
                                    Sludge Cake
                                    after Dewatering
                                    Input Sludge from Treatment Plant
                                    Flow
                                    Meter
House Water
                              Fig. 5-Schematic of system set-up

-------
LONG ROAD SEWAGE PLANT FACILITY

Available for the study of municipal sludges was a Westlnghouse operated
test facility, shown in Figure 6, located at the Long Road Municipal Sewage
Treatment Plant.  The plant, located in Perm Hills, Pennsylvania, uses the
spiral diffused aeration activated sludge process to treat 1 mgd (4 million
liters/day) of municipal sewage.  Figure 7 is a schematic of the treatment
process and illustrates the flow of waste.  Recycle activated sludge from
the final clarifier is wasted through a primary clarifier.  Sufficient
activated sludge solids are wasted so that a sludge age of three days can
be maintained in the aerator.  The combined sludge solids from the primary
clarifier are digested and dewatered by a vacuum drum filter.  Available
for this study, therefore, for processing by the capillary dewatering unit
were activated, mixed primary, and digested sludges.  Table 1 below lists
the average sludge  characteristics, which were  compiled from data taken
during this test program.  Plant influent BOD and suspended solids averaged
150 and  180 mg/1 respectively.

It should be  noted  that this activated  sludge is relatively high in solids
content.  They  carry  an unusually high  aeration cell miss concentration and
achieve  good  settling  characteristics.  Because of  the high solids content,
the sludge may  be partially  stabilized  aerobically  in the aeration cell
resulting  in  low values of mlvss.  This plant feed  also is  almost exclusively
municipal  in  character with  practically zero industrial load which may  account
for  the  relatively  low dissolved solids level.   Tap water TDS  in this area
normally is  in  the  range  of  200  mg/1.
                                   Table 1

Total solids (mg/1)
Total volatile
solids (mg/1)
Dissolved solids
(rag/1)
Dissolved volatile
solids (mg/1)
PH
Sludge specific
resistance
(sec2/gm) x 10~8
Sludge type
Activated
19,545
10,620
840
200
6.9
17.3

Mixed
primary
40,480
23,310
1,572
646
6.3
40.0

Digested
48,235
23,425
1,280
860
7.1
3.89

                                    -  10  -

-------


Fig. 6 - Westinghouse test facility at the Long Road Sewage Plant

-------
NJ

I
                               Anaerobic
                                 DFgester
                               1st Stage
                              Preaeration
                2nd Stage
                       Sludge
                      Holding
                                         Aeration Tank
                             Chlori nation
                                Tank
         Com mm uter
                              Secondary
                               Clarifier
                            Aeration Tank
                                                                                        Vacuum
                                                                                         Filter
Return Activated Sludge
Waste Activated Sludge
                     Filtrate From Vacuum Filter
:Treated Water
                                                             To Stream
                           Fig. 7-Long Road Sewage Treatment Plant - flow schematic
  Waste
  Solids
"Trucked
  To Land
  Fill

-------
To further characterize these sludges, specific resistance determinations
were made on each sludge type according to the procedure described in
Reference 6.  The specific resistance values recorded in the table above
are for no coagulant addition.  Figures 8, 9, and 10 show the specific
resistance values of these sludges as a function of coagulant dosage.
Several different coagulants were evaluated.  This data was used to set
approximate coagulant levels for the sludges used in tests on the capillary
dewatering device.

BELT-LIFE TEST APPARATUS

As part of this program, a continuing life test evaluation on several swatch
samples of different porous media was made using the apparatus shown in
Figure 11.  Photographs of the swatch test samples are given in Figure 12.
The various samples were attached to the endless metal belt.  The apparatus
was partially filled with activated sludge (about 0.3m depth) and the swatch
samples tracked through the sludge.  The sludge was continuously aerated and
also changed approximately every three days.  A small compression roller was
situated such that each swatch sample would pass under the roller and be
slightly compressed.  This was done in order to approximately simulate the
mechanical loading expected in the actual capillary dewatering device.  This
test apparatus was operated about one year.

TEST PROGRAM AND PROCEDURE

The test program on the pilot scale capillary dewatering unit was conducted
at the Westinghouse facility located at the Long Road Sewage Plant.  This
test program included operation of the capillary dewatering device on activated,
mixed primary-activated, and anaerobically digested sludges.  The experimental
design was organized such that an overall machine performance and operation
could be determined as well as an evaluation of specific system operating
parameters such as coagulant dosage effects, belt speed, roller compression
force, etc.  Day to day test runs generally lasted from 2 to 6 hours.  More
than 300 total hours were accumulated in the operation of the test unit.

Start-up procedure involved preselecting belt speed, sludge feed rate, and
coagulant dosage.  The compression roller force was selected (except in
certain specific tests) such that satisfactory operation of the compression
station could be maintained.  This generally involved manipulating the roller
spring deflection to achieve the best cake detachment efficiency possible,
while, at the same time, obtaining the highest cake solids.  These judgements
were based on prior experience.

Test data was taken only after sufficient time (usually 15 to 30 minutes)
was allowed for attaining equilibrium operation.  This same procedure for
data taking was practiced whenever any of the operating parameters were varied.

Routine test measurements included sludge feed rate, coagulant  feed  rate,
sludge cake dry solids, screen wash water flow rate, cake  filtrate flow,  and
compression roller spring deflection.  In addition, the feed sludge  was sampled
and analyzed for  total, volatile, dissolved  solids and dissolved  volatile
solids.  These constituents were analyzed in accordance with procedures outlined
                                     -  13  -

-------
                             Total Solids  Coagulant  Date
                             18(400mg/je    C-31   10/71
                             23,300mgft    C-31    8/71
                             15,800mg/l     FeCf     2/72
CXJ
   2X10
             2    4     6    8    10    12    14    16   18   20
                   Coagulant Concentration (Ibs/ton)
                       C-31 Polyelectrolytex 1.0
                        FeCI3 x 10-1


         Fig. 8-Sludge specific resistance - waste activated sludge
                       (Kgs/tonlm) =2.0 Ibs/ton)
                                -14 -

-------
CM
   O)
   o
   c
   ro
   U
   O>
         10
          8
          6
           8
         10
           7
                                Total Solids
                                38,739 mg/l
                              Coagulant
                                ST-260
                             Polyelectrolyte
                        Date
                        9/31/71
I   , I	L_l
J	L
             0   5   10   15   20  25   30   35   40   45  50
                     Coagulant Concentration (Ibs/ton)

             Fig. 9-Sludge Specific Resistance - Mixed Activated - Primary
                               (Kgs/ton(m)=2.0 Ibs/ton)
                                 - 15 -

-------
CVJ
  
   c



   CD

  ^U

  *o
         10
          8
          6
           10
10
 8
                       Total Solids
                       35,476mg/e
    Coagulant
      ST-260
    Polyelectrolyte
      Date
      9/31/71
                                   J_
                              1
J	L
J
           0    5   10   15   20  25   30   35   40   45  50
                    Coagulant Concentration (Ibs/ton)

        Fig. 10-Sludge Specific Resistance - Anaerobically Digested
                       (Kgs/ton)m)=£0 Ibs/ton)
                            -16-

-------
Fig. 11 - Endless belt life test apparatus for evaluating porous
          media swatch samples.

-------
                          1
 t
£

                           Fig. 12 - Porous media swatch samples before entering sewage.

-------
 Date:12/4/72
     Sludge Characterization

 Type sludge   Activated

 Total solids   19.500 mo/1
Run: 1204
Cross Reference Nos.: 1766190-91
         Machine Parameters

    Sludge feed rate   6.5 1/min
 Total dissolved solids   9800 mg/1
 Dissolved solids    800 mg/1
    Belt-sludge contact time   3.5 sec.

    Coagulant type	C-31
 Dissolved volatile solids   125 mg/1
 pH    6.9	
    Coagulant concentration
    Run time
                                                                                      18.7 ///ton
                start  217.7   finish  219.2
Sample
No.
930
931
932
933
934
935
936
937
938
939





*Roller st
Inches
Along
Belt
5
10
15
20
25
30
35
40
50






mple for tc
Sludge Cake Dewatering
Characterization A
Before After Other
Comp . Comp . g/mln
T.S.
5.9
8.3
9.8
10.4
10.6
10.7
11.0
11.0
11.0






tal soli
T.S.









14.5





ds balanc
T.S.









112.8





e.
Filtrate
Characterization
Belt Water Screen Wash
Water
SKffii,
6.4
6.4
6.4
6.4
6.4
6.4
6.4
6.4
6.4
6.4






T.S.








2920







Quan.
tt/min.
















T.S.
















Machine Performance
Solids Loading
(Ibs/ft2)

.0045
.0045
.0045
.0045
.0045
.0045
.0045
.0045
.0045
.0045






Solids
Recovery
%








88.6
92.2






Solids Loading
Rate
(Ibs/hr ft2)








4.63
4.63






    Compression Roller
Load—in. deflection in springs  1/2 Inch (12.4 #/in)
Pickup efficiency	
           Belt squeegee_
NOTES:  300 mesh screen
                                  Table 2 - Sample Data Sheet (after sample analysis)

-------
in the Standard Methods for the Examination of Water and Wastewaters or
EPA approved alternate methods.  Sludge pH was also occasionally monitored.
A sample data sheet is shown in Table 2.  The cake solids capture (indicative
of cake process water quality) was determined by two methods; first by
determining for a given time increment the actual dry sludge solids discharged
from the compression roller and comparing this with the measured solids in
the feed stream, and secondly by calculating cake solids capture from a mass
balance on the feed stream, sludge filtrate and wash water flows.  These
two methods generally agreed to within a few percentage points.

An estimate of the error involved in the measurement and reproducibility of
each of the basic  test parameters is given in Table 1-A in Appendix A.  The
cumulative effect  of  these  errors on the various  calculated  quantities is
given  in Table 3 below.  Further  discussion of  the error analysis procedure
including some sample calculations is  also given  in Appendix A.
         Table 3.   EXPECTED UNCERTAINTY IN THE CALCULATED QUANTITIES
              Parameter
Typical value
      1.   Sludge feed rate

          a.  Activated sludge

              Activated sludge

          b.  Digested sludge

          c.  Mixed primary

      2.  Machine capacity

          a.  Activated sludge

              Activated sludge

          b.  Digested sludge

          c.  Mixed  primary

       3.  Solids capture

           a.   Activated  sludge

           b.   Digested sludge

           c.   Mixed primary

       4.  Coagulant concentration

           Level
2.4 1/min

6.5 1/min

3.0 1/min

3.5 1/min



2.0 Ibs/hr  ft2

5.0 Ibs/hr  ft2

 5.0 Ibs/hr  ft2

 5.0 Ibs/hr  ft2



 90%

 85%

 85%

 4 Ibs/ton

 (2 Kg/metric ton)
Expected maximum
   deviation
     ±2.4%

     +3.5%

     +6%

     ±6%



     +4.1%

     +4.8%

     +7%

     +7%
      +5.3%
      -4.1%
      +7%
      -6.4%
      +7%
      -6.4%
      +10%
        (1  Ib/hr  ft2 21 5 Kg/hr m2)
                                      - 20 -

-------
                                 SECTION IV

                            DISCUSSION OF RESULTS


SUMMARY OF CAPILLARY SUCTION DEVICE SYSTEM PERFORMANCE

The performance of most mechanical sludge dewatering devices is measured by
at least four parameters; system capacity (Kgs d.s./hr m^), final cake solids
(%), solids capture (%) and total costs ($/Kgs d.s.).  Following the convention
used for rotary vacuum belt filters only the working area of the belt is used
in the calculation of machine capacity.

Sufficient test data has been generated from this program, both from the small
lab test unit and from the larger pilot unit, to indicate how these specific
performance parameters are influenced by changes in the various operating and
machine design variables.  For example, trends have been determined indicating
how certain screen parameters affect sludge solids capture and therefore
coagulant costs or similarly, how the sludge solids loading affects dewatering
rate and thus machine capacity.  A summary listing of all the data obtained
from the pilot unit is given in Tables 1-B through 4-B in Appendix B.  These
data reflecting these parametric interactions are discussed in subsequent
sections of this report.  However, before examining this data, a general
summary of machine performance is presented in order that the overall program.
results can be succinctly identified.

Table 4 below summarizes the performance data obtained with the pilot test unit
while operating at the Long Road Sewage Plant on waste activated, anaerobically
digested, and a mixed primary/activated sludges.  This unit was operated for
approximately nine months and more than 300 actual operating hours were accumu-
lated during this study.
     Table 4.  SUMMARY OF PILOT PLANT CAPILLARY DEWATERING SYSTEM PERFORMANCE
Sludge type
WAS
WAS

WAS
WAS

WAS

DIGST

MIXPRIM

Machine capacity
(Ibs/hr ft2)
2.0
2.0
Coagulant
cost
($/ton)
0
4.00
Final cake
solids
(%)
16-19
17-19
(C-31, Polyelectolyte)
3.0
4.3
0
6.40
16
15
(Ferric Chloride)
4.5
4.00
14-15
(C-31, Polyelectrolyte)
5.2
10.00
16-18
(Ferric Chloride)
5.4
(Fe
10.00
rric Chloric
14-15
e)
Solids
recovery
«>
60-75
95

50-65
91

80

88

85

     (Kgs/m2 = 0.205 lbs/ft2)
     ($/Ton = $1.I/metric ton)
                                      - 21 -

-------
 The results  recorded in Table 4  typify  machine performance  on  the various
 sludge types at  several coagulant  dosage  and  sludge  feed  rates.  The  cost
 figures reported in the table represent coagulant  requirements only since
 the capital  and  operating  costs  of this test  unit  are  not indicative  of  a
 full scale system.   Estimates of this cost  for a full  scale system are given
 in Appendix  C.   Coagulant  costs  were  taken  as $.AO/lb  ($.88/Kg)  for the  poly-
 electrolyte  and  $.05/lb ($.ll/Kg)  for the ferric chloride.

 As shown in  the  table,  the test  unit was  operated  both with and  without
 chemical conditioning.   With  the activated  sludge  at a feed rate of 2.0  Ibs
 d.s./hr ft2  (10  Kgs/hr  m2) and a coagulant  demand  (polyelectrolyte C-31)
 corresponding to $4.00/ton d.s.  ($4,40/metric ton),  final cake solids ranged
 around 18 percent with  solids recovery  as high as  95 percent.  An 18  percent
 cake represents  about a 90 percent reduction  in the  sludge  volume and a  cake
 of "truckable" consistancy.   Final cake solids did not appear  to depend  signifi-
 cantly on coagulant addition  but did  decrease slightly when the  machine  feed
 rate was increased  from 2.0 to 4.6 Ibs/hr ft2 (10  to 22 Kgs/hr m2).   Cake
 solids recovery,  however,  was found to  depend strongly on coagulant addition
 and to a lesser  extent  on  feed rate.  With  no coagulant addition, solids
 recoveries were  found to vary from 60 to  75 percent  at the  lower feed rates
 and measured as  low as  50  percent  at the  higher rates. With coagulant addition,
 cake solids  capture improved  dramatically;  to 95 percent with  the polyelectrolyte
 at the lower feed rates.   Comparable solids recoveries are  possible at the high
 feed rates but at an increased coagulant  cost.

 In general,  it was  found that the  ferric  chloride  coagulant yielded better
 overall performance i.e.,  dryer  cake and  better cake detachment  than  the poly-
 electrolyte.  To  achieve comparable solids  recoveries  with  the ferric chloride
 conditioner,  dosage rates  around 200 Ibs/ton  (100  Kgs/metric ton) are indicated.

 Reported data on  the mixed primary-activated  sludge  was limited  to just  one feed
 rate and only the ferric chloride  conditioner.   A  final cake containing  15 per-
 cent solids  with  85 percent solids recovery was achieved.   This  is a  ferric
 dosage rate  of 246  Ibs/ton (123  Kgs/metric  ton)  with a machine loading of 5.4
 Ibs/hr ft2 (26 Kgs/m2 hr).
                                                                              2
 With the anaerobically  digested  sludge, and a machine  loading of 5.4  Ibs/hr ft
 (26  Kgs/m^ hr), solids  recoveries  in excess of  90  percent were attained with a
 ferric  chloride dosage  of  approximately 300 Ibs/ton  (150 Kgs/metric ton).  The
 final  cake solids varied from 16-18 percent.   Assuming a 5  cent/lb (11 cents/Kg)
 cost  for the  ferric chloride,  chemical  costs  for dewatering the  mixed primary and
 the  digested  sludges  ranged from $10.00 to  $15.00/ton  ($11  to $l6/metric ton),
 respectively.

 Further  consideration is given to  the test  data in Table 4  in subsequent sections
where  it  is shown how the machine capacity, final  cake solids and cake capture
 relate  to the various machine  operating and design variables.  Test data obtained
 from  the  smaller  lab unit  and  from the belt life test  unit  is also discussed.
                                       - 22 -

-------
MACHINE DESIGN AND SYSTEM CAPACITY

The physical size of this dewatering device is obviously determined by the
physical size of the capillary zone.  Thus, the efficiency of the capillary
dewatering in forming the sludge cake represents an important design consider-
ation.  With activated sludge, it has been learned through experience that an
8 percent (solids) cake is needed at the end of the capillary zone before
passing into the sludge compression zone.  With wetter cakes, operational
problems with the compression roller may be encountered.  Some examples of
quantitative measurements made of cake formation along the capillary zone are
given by the sludge dewatering curves shown in Figure 13.  The data is for a
waste activated sludge with 2 percent solids that was conditioned by the
addition of 40 mg/1 of a cationic polyelectrolyte.  This data was obtained by
determining the cake solids from sludge samples taken at various positions along
the length of the capillary section of the small test unit.  Two sets of data
are shown, one for a solids loading of 0.005 lbs/ft2 (0.024 Kgs/m2) and the
other for a loading of 0.012 lbs/ft2 (0.58 Kg/m2).  As seen, the two sets of
data exhibit a similar trend in that the rate of water extraction is highest
initially and decreases exponentially as the sludge becomes concentrated.  The
curve for the lower solids loading shows a 10 percent cake is achieved in less
than a 10 second sludge-belt contact time while an 8 percent cake in 20 seconds
is indicated for the higher solids loading condition.  Thus, both the cake
solids and the time needed to dewater the sludge depend on the sludge solids
loading.  A system optimization must consider therefore both these parameters.

By developing a family of these sludge dewatering  curves, a basis was established
for designing and operating the capillary section  of the machine.  The results
of this data for the activated sludge is given by  the curve in Figure 14.  This
curve shows machine capacity as a function of solids loading.  The curve is for
a 2 percent waste activated sludge conditioned with 40 mg/1 cationic polyelect-
rolyte and, furthermore, assumes an approximate 9  percent cake at the end of
the capillary section.  This curve was developed from data obtained from the
small lab unit while the data points shown represent actual operating data from
the pilot unit.  The majority of these data points reflect machine performance
using the polyelectrolyte conditioner.   One data point is shown however, in which
the ferric chloride conditioner was used.

The data in Figure 14 show that the highest machine capacities are achieved at
the lowest solids loading i.e., when the sludge is applied in a very thin layer.
Rates in excess of 6.0 Ibs/hr ft2  (30 Kgs/hr m2) are indicated corresponding  to
a solids loading of 0.004 lbs/ft2  (0.019 Kgs/m2).  It was found, however, that
when  the solids loading was decreased below 0.003  lbs/ft2  (0.014 Kgs/m2)  the
sludge  layer was so thin that it would not distribute uniformly over the screen
belt  and therefore surface area utilization was diminished.  This would  represent
then  a  lower operational limit on the sludge solids  loading.  An upper operational
limit on solids loading occurred when the  sludge  layer became too  thick  to be
effectively compressed by the roller.  This occurred at  about a  loading  of 0.03
lbs/ft2  (0.15 Kgs/m2).

-------
16

14
 0
                         Solids Loading
                         0.005 (Ibs/ft2)
                                      Solids Loading
                                      0.012 (Ibs/ft?)
                           Sludge:  Waste Activated
        10            20            30
         Belt-Sludge Contact Time (sec)

Fig. 13- Sludge capillary dewatering curves
      z             z
40

-------
   7.0
   r5.0
 §4.0
 s.
 CO
   2.0


   1.0
                           FeCI3 -  127 IbsAon
                           Curve Developed from
                            Lab Test Unit,  Fig. 2
                           operating Data from Pilot
                            Unit,
                           Polyelectrolyte  - 4.0|bs/
                            ton
0.005     0.010     0.015     0.020      0.025
             Solids Loading (Ibs/ft2)
                                                                0.030
Fig. 14- Capillary dewatering-machine capacity with waste activated sludge
(kgs/m2=0.205 Ibs/ft2, kgsAon(m) =2.0 fos/ton)
                                  -25 -

-------
Of fundamental importance, the curve in Figure 14 shows that the actual
capillary dewatering phenomena is governed by several different rate limiting
mechanisms which depend on the sludge solids loading.  At very low solids
loadings the sludge cake is thin and its resistance to dewatering is minimal.
Hence, the controlling factors are the rate at which water is absorbed by
capillary action into the belt and the total quantity of water that must be
transferred.  As the solids loading is increased (i.e., a thicker sludge cake),
the cake resistance per unit of belt surface area increases in greater propor-
tion than the solids weight.  Therefore, the dewatering rate decreases.  This
continues until a point is reached where a pore flow is established in the
cake and further increases in solids loading no longer produce a proportionate
increase in cake dewatering resistance.  This represents the minimum point
observed in the curve.  Further increases in solids loading i.e. increase in
dry solids weight, result in increasing machine capacity.  This continues until
the hydraulic capacity of the porous belt is exceeded.

Sufficient data was not obtained to develop design curves for the mixed primary
and the digested sludges.  It can be argued, however, that the design curve
for these sludges should be very similar to that of activated sludge if these
latter sludges are similarly conditioned i.e., conditioned to allow free water
drainage.  This observation is somewhat supported by the limited data that was
obtained for the mixed primary and the digested sludges as seen when these data
are compared with curve developed for the activated sludge case, Figure 15.  The
significance of this result is that the design of the capillary section may be
independent of the initial solids concentration of the sludge providing (1) that
the system can be designed to handle the water hydraulics at the desired solids
loading and (2) the free water in the sludge can be extracted by capillary forces.
The first qualification applies to very dilute sludges while the second is a
limiting condition on the more concentrated sludge types.

The practical utility of the design curve in Figure 14 is two fold; first it
serves initial design purposes for determining the physical size of a unit for
a given plant size and secondly, the curve can be used to adjust machine
operating conditions i.e., belt speed to maximize capacity in any off-design
condition.

The relatively high machine capacities that are indicated by the data in Figure
14 are the result of minimizing cake dewatering resistance by controlling sludge
solids loading i.e., cake thickness.  Another method of decreasing cake resis-
tance and therefore increasing machine capacity is by increased coagulant dosage.
This is seen from the data given in Figure 16 where the capacity of the pilot
test unit was determined as a function of coagulant dosage for a fixed solids
loading.  The reference data points, shown unshaded, are machine capacities
calculated by sampling the sludge layer at different positions along the length
of the machine and determining the effective belt surface area needed to dewater
the sludge to about a 9 percent cake.  This is the same basis used to develop
the curve in Figure 14.  The results from Figure 16 show that when coagulant
dosage is increased from 4 to 20 Ibs/ton (2-10 Kg/metric ton) of the polyelec-
trolyte, machine capacity is increased from 4.6 to a maximum of 8.0 Ibs/hr ft
(40 Kgs/hr m2) but a further increase in coagulant diminishes capacity.  Likewise,
                                      - 26 -

-------
   7.0


   6.0


   5.0
  3.0
U
03
Q.
co
O
Q)

  2.0
   1.0
— Curve Developed from
    Lab Test Unit, Fig. 2.

• Operating Data from Pilot
    Test Unit, Anaerobically
    Digested  Sludge, FeCL
    at  170  Ibs/ton

• Operating  Data from Pilot Test
    Unit, Mixed Primary,  Fed
                                 at 172 Ibs/ton
                                                         3
          Note:  Capillary Dry Cake
          Solids Ranging from 9.5 to 11.5
              0.005     0.010      0.015     0.020
                          SolidsLoading(lbs/ft2)
                                                       0.025    0.030
       Fig.  15-Capillary de watering - comparison of digested and mixed
       sludge data with design curve for wasted activated sludge
           (Kgs/m
                 2
                           Ibs/ft, Kgs/ton(m) =2.0lbs/ton)
                                -27-

-------
11

10
 9
 2

 1
                         Sludge: Waste Activated
                  Solids Loading: 0.0046 (Ibs/ft?)
                      Coagulant: Polyelectrolyte-
                                 Cationic
Note:  Calculations Based on a Sludge
      Cake Dry Solids of 9 Percent.
           10        20        30       40
                Coagulant Concentration (Ibs/Ton)
                                          50
60
    Fig. 16- Capillary dewatering - calculated machine capacity
    (kgs/m2 =dW5 bs/ft2, kg$/ton
-------
a decrease in coagulant concentration from 4 Ibs/ton  (2 Kg/metric ton) to
zero decreases machine capacity to 3.0 Ibs/hr ft2 (15 Kgs/hr m2).

Similar data obtained in a second series of tests would indicate that an even
more dramatic increase in machine capacity can be realized by increasing
coagulant dosages.  Capacities more than twice those suggested by the data
in Figure 16 were calculated i.e., capacities as high as 20 Ibs/hr ft2 (100
Kgs/hr m ).  In this second case, the basis for the calculation was an 8
percent cake at the end of the capillary section.  This calculated data is
shown in Figure 17 for both the use of polyelectrolyte and ferric chloride.
It must be cautioned that the calculated quantities are based on sludge samples
taken along the length of the capillary zone.  Because of the expontial nature
of the sludge drying curves (see Figure 13) relatively small discrepancies in
the cake solids near the equilibrium value can represent large incremental
changes in the equivalent length of the capillary zone.  This length value
figures directly into the capacity calculation.  Actual operating data at
these high capacities is needed to verify the calculations.

A similar trend with coagulant dosage and machine capacity was obtained for
the mixed primary and the digested sludges, Figures 18 and 19.  In these cases
a maximum four fold increase in machine capacity was calculated.

All of the above data were obtained for a relatively low solids loading.   The
effect of coagulant dosage on capacity at a higher solids loading is unknown.
Thus, data at other sludge solids loadings with and without chemical additions
is needed to determine how these curves are affected.  This information would
provide then a more comprehensive basis to optimize machine capacity.  Further-
more, it remains to be determined if the reduced capital cost realized by
doubling the machine capacity with large coagulant addition exceeds the higher
chemical costs.

The behavior of machine capacity with coagulant concentration is not unlike that
observed with the sludge's specific resistance (a measure of sludge dewaterability).
During the course of this investigation, the specific resistance measurements
were made for each sludge type and the data are presented in Figures 8, 9, and
10.   The data for the mixed primary and the digested sludges were obtained after
the sludges had been conditioned with a polyelectrolyte coagulant.   As can be
learned from the figures, increasing the coagulant concentration improved
dewaterability in each case i.e., decreased specific resistance.  This suggests
then, that the data reported in Figures 17, 18, and 19 can be combined using
specific resistance as a normalizing parameter.  Such a correlation was made
for activated sludge using the data obtained for both the C-31 polyelectrolyte
and the ferric chloride i.e., the data from Figure 17.  The results are shown in
Figure 20 where the machine capacity (Ibs/hr ft2) is plotted against sludge
specific resistance.  Based on the limited data obtained, it appears that machine
capacity can be directly related to sludge specific resistance for learning the
effect of increasing coagulant dosages.  A similar comparison for the other two
sludge types could not be made, since specific resistance values were not determined
for the use of ferric chloride with these sludges.
                                       -29-

-------
   30
Sludge: Waste Activated
Solids Loading: 0.0046fbs/«
Coagulant •   poJyelectrolyte
          A   Fed3
   20
15
QC
    10
                            Note:  Calculations Based on a Sludge Cake Dry Solids of 8 Percent
                      100            200              300              400
                      10              20              30              40
                                          Coagulant Addition  (Ibs/ton Dry Solids)

                               fig. 17-Capillary dewatering - calculated machine capacity
                                        2 = 0.205lbs/ft2, Kgs/ton(m) =^0Ibs/ton)
                                                                          300
                                                                           50
600FeCL
 60C-3I

-------
                             Sludge: Anaerobically Digested
                             Solids Loading:  0.006lbs/ft2
                                Coagulant:  Fed.
9
8
7
6
5
4
3
2
1
Note:  Calculations Based on a Sludge Cake
       Dry Solids of 10 Percent Before Roller
          100      200     300      400     500
               Coagulant Concentration (Ibs/ton)
                                             600
700
   Fig. 18-Capillary de water ing - calculated machine capacity
     (Kgs/m2 = 0..205 Ibs/ft2, Kgs/ton (m) =2.0 Ibs/ton)
                           - 31-

-------
20
CM
 IE  15
  i/i
  CO
  a-
  o
  o>
  .£  10
           Sludge:  Mixed Waste Activated and Primary
           Solids Loading:  0.006Lbs/R2
           Coagulant:
                                  Note:  Calculations Based on a Sludge
                                        Cake Dry Solids of 9 Percent
                                        Before Roller
                                        i	I	

                       100             200             300
                           Coagulant Concentration (Ibs/ton)

              Fig.  19-Capillarydewatering - Calculated machine capacity

                   (Kgs/m2 = 0.205 Ibs/ft2,  Kgs/ton (m) =2.0 Ibs/ton)
                                                                   400
                                      -32-

-------
    26


    24


    22
 ~ 20
esi^

 £ 18


 Il6
 >%
  O
 O
    12


    10
  £  8
  CO
     6


     4


     2


     0
       Sludge:  Waste Activated
       Solids Loading:  0.0046 Ibs/ft2
       Coagulant
                 * FeCI3
                 • Polyelectrolyte
 Note: Machine Capacity Based on an 8 Percent Cake
—    Solids Before Roller
                          1
                                       1
                   10
                          20
                                       30
                                  —8     2
      Sludge Specific Resistance xlO   (Sec /gm)


Fig.  20-Correlation of machine apparent capacity with
sludge specific resistance for two coagulant types

              
-------
A second consideration in the design of the capillary section is selection
of  the porous belt material.  One parameter that was expected to affect cake
dewatering is the belt average pore size.  Decreasing belt pore size theoret-
ically increases the capillary pressure and therefore produces a dryer sludge
cake.  Experiments were conducted to simulate the capillary dewatering section
using sintered metal plates in which the pore sizes could be accurately con-
trolled.  The test apparatus is shown in Figure 21.  Five such plates were
tested corresponding to pore sizes of l/2)j, 5y, lOy , 40y and lOOy (y= micron).
These results are shown by the solid curve in Figure 22 where the sludge cake
solids after 2.0 minutes dewatering (sufficient time to attain the final
equilibrium) are plotted against pore diameter.  The data is for a fixed sludge
solids loading.  The curve shows that final cake solids increased with decreased
pore sizes, as expected, as long as the pores were above a lOy size.  Below 10u,
however, final cake solids decreased markedly.  At these lower pore sizes,
surface effects apparently inhibited wetting of the pore spaces and the capillary
action was diminished.  Thus, there is an optimum pore size (about lOy) for
obtaining maximum cake solids.  This maximum was about a 12 percent cake for the
particular solids loading indicated.

In  addition to the sintered metal plate data, data from three other porous
media materials are included in Figure 22.  This data falls in line with the
porous plate results.  In view of the only slight improvement In sludge cake
solids with the denser porous media and since an 8 percent cake at the end of
the capillary section is satisfactory for machine operation, pore size alone is
not an overriding consideration in specifying belt requirements.  Pore sizes of
lOy or greater are adequate.  It should also be noted that denser porous material
(smaller pore size) costs more.

A third consideration in designing the capillary section is belt material
integrity i.e., belt life.   Two factors have been considered; (1) belt structural
strength and (2)  belt biological stability.  The mechanical tensile strength of
the porous belt is maintained by inlaying a "scrim" ( a reinforcing plastic or
cloth screen) along the length of the belt.  Figure 23 shows a photograph of one
felt porous belt and reinforcing scrim.  This scrim serves as the load carrying
member and will tolerate tension loads as high as 2500 psi without failing.

To evaluate the biological stability of various porous belt materials, swatch
samples of these belt materials were attached to the tracking belt of the life
test unit (Fig.  11) and allowed to interact with activated sludge.  A small
mechanical compression load was also applied to each swatch sample in an attempt
to simulate the mechanical-biological interactions that would occur in the
operation of the capillary dewatering machine.  Five different basic types of
porous materials  were initially selected for evaluation.  They were polypropylene
felt, wool felt,  polyurethane foam,  dacron felt and a rayon viscose felt.
Several grades of the different felts and foam were tested, totaling some 15
swatch samples altogether.   A photograph of the five basic porous material types
before testing began and after 30 days is shown in Figure 24.  Shortly after the
first 30 days, both the rayon viscose and wool felts were destroyed i.e..
completely fell apart.  At this time, a nylon felt was substituted.  A plctorical
history of the remaining swatch samples is given in Figs. 25 and 26 which show

-------
                   Plexiglass
                     Mold
Sludge
co

i
                                                                                    Screen
     Fig.21- Schematic arrangement of swatch test apparatus for simulating capillary dewatering
     (cm = 0.3937 in)

-------
      16

      15
1 1 10
       A
   >»  6
   jro
   •a.  ^
       2-
                     , i
•    I  I  I  I I III  I    I   I  I  I '  ••

          Sludge.-  Waste Activated
   Solids Loading;  0.013 (Ibs/ft2)
      o  Sintered Metal Plates
      •  Material I5p,  Foam
      •  Material 70p,  Polypropylene
      A  Material 100M, Nylon
0.2     0.5   1.0
                            I       5     10    20
                             Belt Pore Size (micron)
                            50    100  200
      Fig. 22 - Belt pore size effect on capillary dewatering cake solids
      (kgs/m2=0.205»bs/ft2)
                                 - 36-

-------
Fig. 23 - Porous felt and reinforcing scrim.

-------

             POLYPROPYLENE
CO
CD



                                                    AFTERI30  DAYS IN SEWAGE
                                                   POLYURETMANE FOAM
                           Fig.  24 - Five basic porous material swatch samples before
                                      and  after 30  days testing.

-------
                    I
  POLYPROPYLENE
POLYURETHANE  10/50
                           POLYURETHANE 10/900
                                                        POLYURETHANE  3/900
                                                             CAPILLARY MEDIA
                                                          SWATCH SAMPLES  FROM
                                                          LIFE TEST APPARATUS
                                                            AFTER 3.5 MONTHS
                         POLYURETHANE FOAM 10/900
                Fig.  25 - Swatch samples  after 3.5  months
                                   - 39  -

-------
  POLYPROPYLENE
POLYURETH»NE 10/50
                       •OL TUBE THANE I O/»00
                                                POLYURETM»N£ 3/900
                                                SWUTCH  StHPLES F H 0 N
                                                  •E TEST »PP»R»TUS
                                                  AFTER 12 MONTHS
                              1NE  F 0« M 10/900
                Fig. 26 - Swatch samples after  12  months

-------
the samples after 3 1/2 and 12 months testing,  respectively.   The  three  felt
materials appear in reasonable shape even after 12  months  but  the  foams  would
probably not be acceptable for use.   Capillary  dewatering  tests  after 3  1/2
and 12 months and a strength test (tension)  after 12 months were performed on
each sample.  Results of the dewatering tests were  inconclusive  but the  data
showed that each of the swatch samples including the foams retained a wicking
capability even after 12 months of testing in the life unit.   It is probable
that 12 months exposure in the life test unit corresponds  to about 24 months
of equivalent operating time on the actual dewatering device.   This extra-
polation is based simply on the number of cycles per day the life test apparatus
imposes on each sample in comparison to the cycles  per day demanded by the
dewatering unit.

Results of  the tension test done on both new and used belt samples (after 12 1/2
months in life test unit) are given in Table 5 below.

                                   Table 5
Material
Polypropylene
Nylon
Dacron
Polyurethane
Tensile strength (ultimate)
New (psi) 12 1/2 mo.
2500
1440
1600
75
800
1200
1000
65
% of Original
strength
32
84
62
86
 It  should  be  noted  that  tensile  strength  measured  reflects  that  of  the  scrim
 support  and not  that  of  the  belt material.   The  polyurethane  had no scrim  support.
 The scrim  materials used for the polypropylene and Dacron  felt materials are
 uncertain  but believed to be polyester.   The nylon material used a  nylon scrim.

 In  addition  to the  life  test evaluations, periodic examinations  were made  of  the
 porous  belt used on the  pilot test unit.   Figure 27 shows  a photograph  taken  of
 the belt after 12 months of  testing with  the pilot unit (approximately  300 hrs
 of  actual  test hours).  Some surface abrasion has  occurred as evident by  the
 partial unstranding of the fibers.  This  has not deterred  machine operation.
 Some discoloration  is also noted.  Based  on this study, it would appear that
 the porous felt belt  materials should endure at  least one  year operation.

 COMPRESSION  ROLLER  DESIGN - FINAL CAKE SOLIDS

 The function  of the compression roller is to:  (1) increase sludge solids  from
 8 percent to  over 16 percent and  (2) detach the  sludge from the screen belt.
 Sludge solids loading (solid weight/unit  area)  and compression roller force
 (force/unit  width of belt) are  two parameters found to influence final sludge
 cake solids.   These effects were measured in separate tests using  the small lab
 unit where the actual roller compression force was directly measured with a
 strain gauge.  These tests were done with the waste activated sludge.  Similar

-------
Fig. 27 - Photograph of porous belt from pilot  unit  after
          12 months of testing.

-------
data was also obtained from the pilot test unit using all three sludge types.
In this case the magnitude of the roller compression force was determined by
measuring the spring deflection (the springs to which the roller is mounted).

It was found that cake solids increased when the compression force was increased
and increased when the solids loading (cake thickness) was decreased.   The
normal force load range studies corresponded to approximately a 15 to  45 psi
average (1-3 atm).  A third parametric effect was also identified which
corresponds to the time of contact between the sludge and compression  roller.
This sludge contact time is directly related to the linear belt speed, roller
diameter and wrap angle between the belt and compression roller i.e.,

                                      = !§.
                                 fceff   V,
                                         b

where   t ,.,. = contact time between the sludge and roller during compression

           r = radius of the roller

           0 = wrap angle

          V,  = linear belt velocity

It was found that by increasing t  ._  (keeping solids  loading  and compression
force constant) a dryer cake was    produced.  Combining  the  three parameters
according to the observed experimental effect, a roller  compression parameter
was formulated that adequately correlates the data.   The  parameter is given by
[F • t   /S.L.] where F is the roller compression force  in  Ibs/in, S.L. is the
sludge   solids loading in lbs/ft2 and t ff  is in seconds.

The correlation established between cake solids and  the  roller  compression
parameter is shown in Figure 28.   In  each case, the wrap  angle  0 was  taken as
20° on the lab unit and 10° on the pilot unit.

The data for the  activated sludge  suggests  that an approximately linear relation-
ship exists between final cake solids and the  roller  compression parameter over
the range of the  test data.  Increasing the  compression  parameter  from 100 to 400
increased cake solids from 14  to 20 percent.

The two single data points shown for  the anaerobically digested sludge suggests
that the correlation developed for  the activated sludge  is  not  applicable to this
sludge.  Only one data point is available for  the mixed  sludge  and  that falls
close  to the activated sludge  data.   This would not  be totally  unexpected since
the greater quantity of the mixed  sludge  is  the waste activated sludge.

One factor which  is not accounted  for in  the compression roller parameter group-
ing is  that of coagulant  dosage.   This effect  is shown separately  for each  sludge
type in Figure 29.  The data shows  that for each sludge  type  even  a marginal
addition of  coagulant will increase  the final  cake  solids.   For example, with  the
digested sludge,  adding 1 percent  (based  on dry  solids weight)  coagulant  the
final  cake solids was  increased  from  13.4  (zero  coagulant)  to 14.8 percent.
However, addition of still more  coagulant  does not  appear to  produce  a proportion-
ate increase in  cake solids.   Thus,  the effect on  cake solids of  addition coagulant
appears  to be significant only at  the lower dosage  concentrations.

-------
  22
  21
  20
2 19
to
1»
^ 17
o 16
CO
£15
  14
  13
  12
 A.  pilot Test Unit, Fig. 3
   *   Waste Activated Sludge,  Polyetectrolyte at 4.0 Ibs/ton
 0:  Lab Test Unit,  Fig.  2
      Waste Activated Sludge,  Polyelectrolyte at 4.0 Ibs/ton
 A:  Pilot Test Unit, Mixed
      Activated - Primary Sludge, FeCI3 at 172 Ibs/ton

 •:  Pilot Test Unit, Anaerobically Digested Sludge,
      FeCI^ at 170 Ibs/ton
              	1	1	1	1—
                        J
                           F= Com p. Force Ibs/in
                            _  rO _ Arc Length
                         eff""  vk    Belt Speed
                                b                2
                        S.L = Solids Loading (Ibs/fH
J.
                      _L
-L
±
              I        2         3

       Roller Compression Parameter
                        S.L.
                               xlO
                                             -1
                                           in  L sec
                         i  -  -  j            lbmft"2
Fig. 28- Capillary dewatering - final cake solids
         (kgs/m2 =0.205lbs/ft2. kgs/ton =2.0 IbsAon)
         (kg/m = .036 Ibs/in)

-------
Ln
 I
   17
   16
   15
   14
   13
2 12
o
s
8
I 17
   16
   15
   14
   13
   12
                                              Sludge:  Waste Activated
                                     -Roller Comp. Force:  12.4 Ibs/in
                                    0    5101520304050
                                        C-31 - PolyelectroJyte (Ibs/ton)
        Sludge:  Waste Activated
Roller Comp. Force:  12.4 Ibs/in
50   100r 200  300  400  500   600
 FeCI3- Coagulant (Ibs/ton)
                                    17
                                    16
                                    15
                                    14
                                    13
                                    12
                                                                              17
                                                                              16
                                                                              13
                                                                              12
                                                                                     Sludge:  Anaerobically Digested
                                                                                     Roller Comp. Force:  12.4 Ibs/in
                                                                                                      I
                                            50   100  150   200  300  400  500
                                               FeCL - Coagulant (Ibs/ton)
                                            Sludge: Mixed Primary
                                            Roller Comp.  Force: 12.4 Ibs/in
                                            _L
                                                               l
                                                                                 0    50  100  150  200   250 300   350
                                                                                        FeCL - Coagulant (Ibs/ton)
                                                     Fig. 29-Effect of coagulant dosage on final cake solids
                                                     (Kgs/m2=0.205lbs/ft2,  Kgs/ton(m) =2.0Ibs/ton)

-------
The significance of the compression roller parameter, aside from correlating
the data from both test units, is that it provides a design "tie-in" with the
capillary section.  Both the solids loading (S.L.) and belt speed are specified
from design considerations of the capillary section.  This leaves only the
roller diameter and compression force to be specified in designing the roller
compression section to achieve the desired final cake solids.

A further consideration in the operation of the roller compression section
involves the preferential adherence of the sludge to the roller.  A photograph
depicting this sludge cake detachment is shown in Figure 30.  Excessive roller
compression force and sludge over-coagulation with polyelectrolyte were found
to adversely effect sludge cake detachment.  High compression forces forced
the sludge solids into the screen decreasing solids capture.  With the higher
polyelectrolyte coagulant dosages, the sludge attained a "tacky" (or slippery)
appearance, and the sludge cake would not adhere to the compression roller
surface.  Other factors that could effect cake detachment include screen material,
weave, and fiber diameter.  These parameters have not been evaluated in this
program.

SLUDGE CAKE SOLIDS CAPTURE

Present practice in sewage sludge dewatering is to normally recycle the process
filtrate back to the head end of the treatment plant.  Thus, high filtrate
quality (low BOD, solids, etc.) is not generally demanded.  However, sufficiently
good solids capture (^85%) is required to avoid the problems associated with
continued recirculation of fine solids.  Ultimately these problems can lead to
deterioration of filter production and inceased chemical conditioning require-
ments .

In the capillary dewatering system, to obtain high solids capture, the sludge
solids must not pass through the screen belt.  Solids passage is controlled by
screen mesh size, sludge floe size, and roller normal force.  The first two
parameters were studied in separate experiments.

The effect of screen mesh size (screen opening) is illustrated by the data shown
in Figure 31.  Four different size screens (100, 200, 325, and 400 mesh) were
evaluated using the swatch test apparatus shown in Figure 31.  Each screen was
evaluated by measuring the weight fraction of solids that escaped the respective
screens when the sludge was applied.  These tests were conducted with waste
activated sludge applied at a relatively heavy solids loading (0.080 Ibs/ft2)
(0.34 Kgs/m2) and conditioned with 4.0 Ibs/ton (2.0 Kg/metric ton) polyelectrolyte.
As the data shows, increasing screen mesh size (decreasing screen opening)
improves solids capture.  This is particularly evident at the higher mesh sizes.
Above 300 mesh, however, there appears to be very little additional improvement
in solids capture with further increases In screen mesh.

Solids capture data was also obtained while operating the pilot test unit with
activated sludge.  This data was taken with machine capacities ranging from 2.0
to 4.6 Ibs/hr ft2 (10 to 22 Kgs/hr m2); coagulant dosages from 0 to over 40 Ibs/
ton (0 to 20 Kgs/metric ton) of a polyelectrolyte; and two different mesh screens
(200 and 300 mesh).   The data is given in Figure 32, which shows sludge cake
                                   - 1*6 -

-------
Fig. 30 - Photograph depicting sludge cake detachment,

-------
  100
TO
O
o
CO
% 90
o
|
             Sludge:  Waste Activated
          Coagulant:  C-31 (Dow) - 4. Dibs/Ton
      Solids Loading,-  0.07 (Ibs/ft2)
                       Data from Swatch Test Apparatus
     50    100
150    200    250    300
        Screen Mesh Size
350    400    450
       Fig. 31 - Effect of screen mesh size on solids capture
       (kgs/m2=0,205 Ibs/ft2,  kgsAon(m) =2.0 IbsAon)

-------
                                                           1
                               Sludge: Waste Activated
                            Coagulant: Polyelectrolyte-Cationic
                                 Machine Capacity  Screen
                                                           •
                            — a -4.6 Ibs/hr ft* - 300 Mesh
                                o -2.0 Ibs/hr ft2-200 Mesh
                                o -3.0 Ibs/hr ft2-200 Mesh'
                            — • -2.0 Ibs/hr ft2-300Mesh"
              10             20             30
                 Coagulant Concentration (Ibs/ton)
40
Fig. 32 -Capillary dewatering - sludge cake solids capture
(kgs/mz =0,205 Ibs/ft2 ,  kgs/ton(m) = 2.0 IbsAon)

-------
  solids  capture  as  a  function  of  coagulant  dosage under various operating
  conditions.  The data  is  for  the polyelectrolyte coagulant only.  The effect
  of screen mesh  size  is as previously predicted  in Figure  31.

  The Improved cake  capture with increased coagulant addition is as expected.
  With no coagulant  addition, cake capture varied from 50 to 75 percent depending
  on the machine  feed  rate and  screen type.  Cake solids captures of 95 percent
  or higher were  achieved at a  coagulant dosage of 10 Ibs/ton (5 Kgs/metric ton)
  or about $4.00/ton ($4.40/metric ton) dry solids.  This is at a machine capacity
  of 2.0 Ibs/hr ft/  (10 Kgs/hr m2) .  Increasing machine capacity to 4.6 Ibs/hr ft*
  (22 Kgs/hr m2)  by  reducing the solids loading (i.e., maintaining a thinner cake
 but increasing  the sludge pumping rate and belt speed) diminshed cake solids
  capture.  This  is  attributed to the fact that a thinner sludge cake is not as
 effective in capturing fines as a thicker cake.   Solids capture can be improved
 at the higher machine capabilities by increasing coagulant dosage.   Thus, a
  trade-off between machine capacity, coagulant dosage and cake filtrate quality
 can be made.

 The data showing cake solids capture for activated sludge  with ferric chloride
 conditioner is  shown  in Figure 33.   The data was taken with the 300 mesh screen
 at a machine capacity of  4.3 Ibs/hr ft  (21 Kgs/m2  hr).   Comparing  this  data with
 the equivalent  data in Figure  32  shows that 90 percent  solids  capture is obtained
 at about a 15 Ibs/ton (7.5 Kgs/metric  ton)  polyelectrolyte while  the equivalent
 solids  capture  for  the ferric  chloride is  obtained  at  130  Ibs/ton (65 Kgs/metric
 ton).   On  a cost basis,  this means  $6/ton  ($6.60/metric  ton)  of dry sludge solids
 to condition with polymer  and  $5.20/ton  (5.72/metric  ton)  to  condition with ferric
 chloride (FeCl3).   On this  basis,  it must be  reasoned  that the ferric chloride
 is more cost effective  than  the polyelectrolyte.  With  the capillary dewatering
 system,  this difference could  be  associated with the  relative  effectiveness  of
 the  two coagulants  in effecting sludge  cake detachment.  The polyelectrolyte has
 an inherent  tackiness which appears  to inhibit cake detachment (cake  tends  to
 adhere  to  the screen  belt) .  This consideration  is  in and  above any  differences
 in the  coagulating  effectiveness  of the  two conditioners.   When comparing  the
 two coagulant systems, these factors must be  balanced against  the larger volume
 of sludge produced  due to  the  addition of significant amounts  ferric  chloride,
 the expense  of handling the larger volumes  of coagulant, and the  corrosive nature
 of ferric chloride  solutions.  Lime may be  added in the plant  to  control corrosion
 and improve  conditioning.

 Solids capture data for the anaerobically digested and mixed primary sludges  are
 shown in Figures 34 and 35.  With digested sludge, solids  captures over  90 percent
were attained at a  coagulant dosage of 300  Ibs/ton (150 Kgs/metric ton).  This
 data is for a machine operating between 5 and 6 Ibs/hr ft*  (24-30 Kgs/m2 hr).
With the mixed primary sludge, the best solids capture achieved was 85 percent.
This is a coagulant dosage of 250 Ibs/ton (125 Kgs/metric  ton).  Both of these
sets of data were attained using ferric chloride conditioner.

GENERAL MACHINE OPERATION

Operation of the capillary dewatering pilot scale test unit has provided sufficient
experience to anticipate potential problems with a full scale system.  The general
operation of the unit  on activated sludge was excellent.  There were no particular

                                    -  50 -

-------
  100
_ 90
#80
to
0>
   70
   60
   30
              -—— ""A""    Sludge.-  Waste Activated
                             Coagulant: FeCL

              Machine Capacity          Screen
               •4.3lbs/hrft2          300 Mesh
                             .2
                                          L 89 Ibs/ hr ft
                                       200 Mesh
 I
I
I
               50
100       150        200        250
     Coagulant Dosage - FeCL (Ibs/ton)
                             300
                             350
400
                      Fig. 33-Capillary dewatering - sludge cake solids capture
                        (Kgs/m2 =0.205 Ibs/ft2, Kgs/ton (m) =2.0 Ibs/ton)

-------
    100
     90
^

OJ
CO
;o

"o
l/>

o>
-a*

5

0>
70
     60
                                  Sludge: Anaerobically Digested
                                  Coagulant:  FeCL
                       Machine Capacity

                       •  5.7lbs/hrft2
                       *  3.2lbs/hrft2
         Screen

       300 Mesh
       200 Mesh
     50
                            1
1
              100          200          300          400
                   Coagulant Dosage - FeCL (Ibs/ton)


          Fig. 34-Capillary de water ing - sludge cake solids capture

            (Kgs/m2 = 0.205 Ibs/ft2 Kgs/ton (m) » 2.0 Ibs/ton)
                                                                      500
                                    .52-

-------
            100
            90
            80
VI
u>
 I
CO
            50
           Sludge:  Mixed Waste Activated and Primary
           Coagulant:  FeCU
           Machine Capacity:  5.2 Ibs/hr ft2
           Screen:  300 Mesh
                                              I
                        30
                          100        150        200       250
                               Coagulant Dosage - FeCI, (Ibs/ton)
300
350
400
                               Fig. 35- Capillary de water ing - sludge cake solids capture
                                        2 = ).205lbs/ft2, Kgsfton(m) =2.0 Ibs/ton)

-------
 problems encountered in pumping the sludge to maintain the uniform and thin
 sludge layers required for the higher machine capacity operation.   The sludge
 cake would detach cleanly (preferentially adhere to the compression roller)
 even over a relatively wide range of compression force settings.   With this
 sludge, the machine could be run unattended for relatively long periods of
 time (several hours).   The ease of operation with the activated sludge is
 attributed to the sludge's homogeneity.   The mixed primary sludge  exhibited
 a similar homogeneity  but was heavier (higher solids content).   This  sludge
 has a strong anaerobic odor making it unpleasant to work with.

 With the anaerobically digested sludge,  pump clogging was frequently  encountered
 because of hair and large solids.   This  problem was circumvented by changing
 pumps.

 With the heavier sludges  i.e.,  both the  mixed and digested sludges,  the compression
 roller  section operation  (cake  detachment)  appeared more sensitive  to change  in
 coagulant dosage,  coagulant  type and roller force.   These are qualitative  obser-
 vations that need  additional investigation.

 The most  serious mechanical  problem encountered  in  operating the pilot  unit was
 maintaining  the  integrity of the screen  belt  for extended periods.  During  the
 early part of  the  program,  frequent screen  failures  were encountered  (after only
 2  or 3  weeks operation).   The screen was  observed to tear at the seam and near
 the edges.   These  screen  failures were not  catastrophic  but gradual.  The failure
 at  the  seam  was attributed  to the method  of  fastening  the screen together.  It
 had been  sewn.  Sewing  the screen actually  put a non-uniform and point  loading on
 the screen fibers.   This  mode of  failure  was  finally corrected by subsequently
 bonding  the  two ends of the  screen  together.  This proved to be an easy and
 effective method of  screen attachment.  The  tears at  the  edge of the  screen were
 eliminated by edging the  screen  (doubling over the screen to put a 1/4  inch edge
 along both sides)  and eliminating screen  contact with  sharp metal edges on  the
 unit.  For example,  the screen guides were  removed and a  teflon edging was put
 on  the underside of  the feed tray.  These changes appeared to signifianntly improve
 the screen integrity during  the remaining portion of  the  test program (about 3
months).  It is not known whether the fine mesh  screens used in this pilot study
would be acceptable in large scale  field systems.  Heavier (large fiber diameters)
screens may be needed for these systems.

Only one porous belt was used during the course of this investigation.  There were
no operating problems encountered with this belt, and the belt,  in fact, still
appears in excellent condition.

Several minor machine operating problems  were encountered and solved during the
 Bourse of this study.  This included some spray water replumbing to prevent water
 -un-back (into the belt) and retracking the screen belt to take  maximum advantage
 f the large  belt area.   The reader is referred to Appendix B, Tables 1 through 4.
 ncluded in the tables  are some  general comments that reflect  some  of the operating
 roblems encountered.

-------
                                SECTION V

                                REFERENCES
1.   Adrian,  D.  D.,  Smith, J. E., Jr.,  "Dewatering Physical-Chemical Sludges,"
    Application of  New Concepts of Physical-Chemical Wastewater Treatment,
    September 18-22,  1972.  Published  in Pergamon Press, Inc., pp. 273-289,

2.   USEPA, "An Environmental Law—The  Federal Water Pollution Control Act
    Amendments of 1972—HIGHLIGHTS," published by Office of Public Affairs,
    U.S.  Environmental Protection Agency,  Washington, D.C., December 1972.

3.   Fowler, G. J.,  "Apparatus  and Method  for Separating  Solids  From Liquids",
    U.S.  Patent 2,021,122,  November  12,  1935.

4.  Zaromb, S., "Apparatus  and Method  for Separating  Slurries  Into  Solid  and
    Fluid Components," U.S. Patent  3,207,061,  September  21,  1965.

5.  Goodman, B. L., et. al., "Sewage Treatment System,"  U.S.  Patent  3,531,404,
    September  29,  1970.

6.  Kline, S.  J.,  and McClintock,  F. A., "Describing Uncertainties  in  Single
    Sample Experiments", Mechanical Engineering, Vol. 75,  1953, pp.  3-8.
                                    - 55 -

-------
                                 SECTION VI
                          APPENDIX A - Error Analysis
The data from any experiment can only be interpreted within the limits of the
accuracy and reliability of the measurements.  These limits are difficult and
often impossible to ascertain in single sample experiments.  Nevertheless, it
is necessary for the experimenter to attempt to describe the uncertainties in
the data in order to add credence to the results.  Such an analysis would first
be extremely helpful in selecting the apparatus best suited for the experiment,
and secondly, give the experimenter a basis for evaluating his data.

An analysis has been conducted to describe the uncertainties in the data reported
herein.  The calculations are based on the equations presented by Kline and
McClintock, (*>) who show that the uncertainty interval Wr in some function R of
n  independent variables V.^  is given by
             W  =
 3V,   2
i   i.
                                                   9V
                                                    n
                        W
                                                         n
                                                             1/2
 where  W,  is  the uncertainty  interval  in the  variable  V...   In  developing  the  above
 equation,  it was assumed that  the  same  odds  exist  for each of the  variable
 intervals  and for the  result i.e., if the  confidence  intervals of  the W^ variables
 are 90 percent, then the confidence interval on W   will also  be 90 percent.   Using
 this equation, the uncertainty in  the variables can be estimated.   The basic
 measured quantities and their  respective uncertainty  intervals are summarized in
 Table  A.I.   The confidence intervals  in the  variables were arbitrarily set  at
 90 percent.   The calculations  for  the error  in the derived quantities are
 summarized below.

         Table A-l.  EXPECTED UNCERTAINTY IN MEASURED VARIABLES
                Quantity
   1.  Belt active length

   2.  Belt active width

   3.  Sludge total suspended solids

       a.  Activated

       b.  Mixed-activated primary

       c.  Anaerobically digested

   4.  Sludge sample weights (gram balance)

       a.  Beaker wt.

       b.  Beaker wt. + wet solids


                                      - 56 -
                Typical value and
               confidence interval
                    50+1.0 inch
                    (cm = .39 in)
                  10.5 + 0.25 inch
                19,000 + 100 mg/£

                40,000 + 400 mg/fi,

                45,000 + 450 mg/£



                   173 +0.1 gm

                   360 +0.1 gm

-------
   Table A-l  (continued).  EXPECTED UNCERTAINTY IN MEASURED VARIABLES
              Quantity
                                            Typical value and
                                           confidence interval
        c.   Beaker wt. + dry solids


    5.   Time measurements  (stop watch)


        a.   Solids capture measurement


        b.   Sludge feed measurement  (low)


        c.   Sludge feed measurement  (high)


    6.   Sludge  volume  measurement (graduate


        cylin.)


        a.   Activated  sludge  (low feed  rates)


        b.   Activated  sludge  (high feed rates)


        c.   Mixed-primary-activated


        d.   Anaerobically  digested


    7.   Chemical feed  rate
                                              200 + 0.1 gm




                                               60 + 1.0 sec.


                                               15 + 0.25 sec.


                                               10 + 0.25 sec.
                                               600  + 10 m&


                                              1000  + 25 mi


                                              1000  + 50 m£


                                              1000  + 50 mi


                                                10+1 m£/min
Experimental Uncertainty in Sludge Flow Rate (W.A.S.)


F.R. = Flow Rate - Sludge Volume/time = S.V./t


     From Equation A-l, the uncertainty in sludge flow rate becomes;


                                              1/2
                WF.R.

                F.R.



Now, from Table A-l,
M
                    ws.v _±io
                    S.V. ~ 600 -
                                       1.7%
                    _
                    t
                              60
                                    +  1.7%
                                                                       (A-2)
                                    - 57 -

-------
            Therefore,  from Equation (A-2),
                                 WF.R.
                                 F.R.
       +2.4%  (low sludge feed rates)
            Similarly, for the high feed rates,

                                 W,
                                  F.R.
                                 F.R.
     = +3.5%
   b.  Experimental Uncertainty in Machine Capacity (W.A.S.)

   ,  ,   „          Sludge Solids Wt x Sludge Feed Rate x Conversion Factory
Machine Capacity = 	B	R2n- AT.-,	
                               or M.C. =
       Belt Area
       S.W. x F.R.
           B.A.
            Thus, the uncertainty in machine capacity is;
                     WM.C.
                     M.C.
S.W.
         F.R.
B.A.
                                                              1/2
                                          W.
                                           B.A.
            The uncertainty in belt area,    '  ',  is given by; B.A.
   width)  thus, from Table A-l,
                                  =  length  x
                        W.
                         B.A.
                        B.A.
  i.or + 1.25
50
           10.5
                                                   1/2
                     = +3.3%
    Thus;  from Table  A-l and above,  (low capacities);
                                                        1/2
                   M. L.
                           [(.005r + (.024)   + (.033r]     »  +4.1%
    Similarly, for the higher capacities,
                                   WM.C.
                                   M.C.
        = +4.8%
                                           - 58-

-------
c.  Experimental Uncertainty in Cake Solids Capture (W.A.S.)

        „ , _,,  _         _ „    Dry Solids From Roller   D.S.R.
        Solids Capture = S.C. = _. ^ g . . ,—	—3— = _ _ _
                 *              Dry Solids From Feed     D.S.F.
Therefore,
                       WS.C.
                       S.C.
        w.
     2   rW   .2
 DSR[    |  DSF
DSR J    [DSF
                                                  1/2
                                                 (A-3)
The uncertainty in the measurement in the dry cake solids from the compression
roller is a result of three factors:

             1.  weighings +0.5%
             2.  sampling time +1.7% (60 second sample with a +1.0
                 second accuracy)
             3.  edge losses +2%  (estimate)

On this basis, then, the uncertainty in the dry cake solids wt.  from  the  compression
roller is,
                                  W.
                                   DSR   -2.2%
                                  DSR    +4.2%

The uncertainty in feed dry solids wt.  is basically  in measurement  of this  sludge
feed rate.
                                 W
                                 WDSF
                                 DSF
                +2.4%
Thus,  from Equation  (A-3),  the uncertainty in cake solids  capture is;
ws.c.
S.C.
                                  (.022)
                                          ,  t
                                  (.042)2  + (-
                                                    1/2
 Similarly,
                                W
        S.C.
       S.C.
                                        +4.9%
                                        -3.2%
             (low feed rates)

                                 b • L* »    "TO * J« /. ,  ,  -  ,    .   v
                                 ^7~ = -4.1% (high feed  rates)
 Similar calculation follows for the mixed activated-primary sludge and for the
 anaerobically digested sludge using the uncertainties given in Table A-l .  The
 results of the calculations are given in Table 3 of the text.
                                    -59-

-------
                                SECTION VII

               APPENDIX B - A Chronological Summary Listing of
                            Test Data—Pilot Test Unit


A summary of test data from the pilot unit is given in Tables IB through 5B.
The data is arranged in chronological order.  Included In each table are CD Run
number which merely corresponds to the date of testing i.e., month and day  (521 ~
May 22) and (2) Type of sludge - ACT - waste activated sludge, DIGST - anaero-
bically digested sludge and MIXPRIM - mixed primary activated sludges.  The
remaining columns are self explanatory.

Table IB summarizes data obtained during the initial start-up and system shake-
down series.  During this time, most of the machine operating problems were
solved and improved experimental methods for obtaining solids recovery values
were developed.  The data is limited to basic machine performance on activated
sludge using one screen type.

Table 2B shows data that reflects a continuation of developing base line system
performance.  Methods for obtaining solids recovery data were Incorporated  during
this time along with attention to measuring roller compression forces.  Initial
data on the digested and mixed primary sludges was also obtained.

Tables 3B and 4B summarize data obtained with activated sludge during that  portion
of the program that involved developing a more basic understanding of various
system parameter interactions.  This included varying coagulant dosage rates,
belt speeds, sludge feed rates, screen type, and roller compression forces.
These sets of data constitute the most reliable and informative compilation of
tests conducted on waste activated sludge during this program.

Table SB summarizes data taken in the anaerobically digested and mixed primary
sludges.
                                    - 60 -

-------
                         Table  1-B   Pilot  Test  Unit  -  Summary  of  Data  From May  22  through Aug.  10,
                                     1972 - System   Installation and  Shakedown
Run
522

524
602
606
607
608
609
612
614
627
628

713
718-A
718
719-A
719
720
720-A



726

728
731
801
802
803
808
809
810


Sludge
Act

Act
Act
Act
Act
Act
Act
Act
Act
Act
Act

Act
Act
Act
Act
Act
Act
Act



Act

Act
Act
Act
Act
Act
Act
Act
Act


Coagulant
Type
None

C-31
FeCl3
C-31
C-31
C-31
C-31
C-31
C-31
Fed 3
FeCl 3

Fed 3
FeCl3
FeCl3
FeCl3
Fed 3
FeCl3
FeCl3



None

None
None
None
None
None
None
C-31
C-31


(Ibs/
ton)
0

17
103
5
5
7
14
1.3
8
28
27

300
95
140
52
270
230
21



0

0
0
0
0
0
0
5
5


Cake
Solids
(%)
13.2

13.5
16.3
16.2
15.9
15.7
15.5
16.4
15.8
17.2
18.4

15.4
17.8
18.1
17.3
20.3
17.4
18.9



17.1

17.0
18.0
16.2
16.6
16.8
16.5
17.5
16.6


Comp .
Force
(Ibs/
in)
_

-
-
-
-
-
-
-
-
-
-

-
_
-
-
-
-
-



-

-
-
-
-
-
-
-
-


Solids
Loading
(Ibs/
ft2)
0.0097

0.0135
0.0121
0.0084
0.0083
0.0091
0.0063
0.0098
0.0110
0.0095
0.0093

0,0066
0.0088
0.0088
0.0081
0.0071
0.0071
0.0082



0.0078

0.0068
0.0081
0.0081
0.0077
0.0077
0.0080
0.0070
0.0070


Machine
Capacity
(Ibs/
hr ft2)
2.32

2,04
2.18
2.52
2.40
2.72
1.89
2.93
1.33
2.83
2.78

1.98
2.65
2.65
2.41
2.13
2.20
2.46



2.44

2,12
2.53
2.62
2.30
2.29
2.60
2.50
2.50


Solids
Recovery
(%)
__

-
-
-
-
-
-
-
-
-
-

-
-
-
-
-
-
*



-

_
-
-
-
_
-
-
-


Run
Time
(hrs)
3.0

3.0
2.5
4.0
4.0
4.0
3.5
4.5
4.5
4.0
2.5

3.0
4.0
3.5
3.0
4.0
4.0
4.0



3.5

4.0
4.5
4.0
4.5
2.0
4.0
3.0
2.5

i
Screen
Type
(Mesh)
200

200
200
200
200
200
200
200
200
200
200

200
200
200
200
200
200
200



*

200
200
200
200
200
200
200
200


Comments
Shakedown - comp . force not
measured


Belt tore at seam — resewn






Changed compression roller -
machined stainless steel.
Chera. feed pump not functioning.
Screen repaired prior to run.
Repaired feed pump.

Comp. roller hanging up.

Screen wash water spilling into
belt effluent stream - All prior
solids recovery data invalid.
Screen tore.
Changed screens - new one 200.
Bonding screen together.

Belt dirty—wash w/ soap & water.



Comp. roller stalling

Changed position of comp. roller.
Re tracked belt.

H
 i
                          (Kgs/ton(m) =2.0 Ibs/ton, Kg/m = 0.056 lbs/in., Kgs/m2 = 0.205 Ibs/ft2)

-------
Table 2-B  Pilot Test Unit - Summary of Data From Aug.  16 through Oct.  4,
           1972 - Base Line System Performance














1
ON
IVk
IV
1


















Run
816

817
818

821
823

824
825
828
829
8 30- A
830-B
830-C
830-D
830-E
908


911

913
913-A
915
915-A
918
919
920-25

927
1003

1004

Sludge
Act

Act
Act

Act
Act

Act
Act
Act
Act
Act
Act
Act
Act
Act
Digst


Digst

Act
Act
Act
Act
Act
Act
Digst

Act
Mix-
Prim
Mix-
Prim

Coagulant
Type
C-31

C-31
C-31

C-31
C-31

C-31
C-31
C-31
C-31
Fed 3
FeCl3
FeCl3
FeCla
FeCl3
Fed 3


ST-260

None
C-31
C-31
C-31
C-31
C-31
ST-260

C-31


C-31


Ibs/
ton)
5

4
3

7
10

19
9
2
0.5
190
95
48
19
9
9


2

0
9
5
6
50
34
2

26
-

5


Cake
Solids
CO
17.6

17.9
17.8

18.6
17.6

19.8
18.3
18.7
19.4
19.3
20.0
19.1
20.2
20.3
20.0


19.9

18.9
18.8
-
-
18.6
19.2
21.2

19.7
-

20.8


Comp.
Force
(Ibs/
in)
18.5

18.5
16.4

18.5
16.4

20.4
18.5
20.4
20.4
20.4
20.4
20.4
20.4
20.4
16.4


-

17.4
16.4
-
-
20.4
20.4
-

20.4
-

-

Solids
Joading
(Ibs/
ft2>
0.0079

0.0088
0.0078

0.0081
0.0078

0.0082
0.0086
0.0078
0.0077
0.0079
0.0079
0.0079
0.0079
0.0079
0.0135


0.0165

0.0085
0.0085
0.0071
0.0071
0.0047
0.0045
0.0011

0.0061
-

0.0084

Machine
Capacity
(Ibs/
hr ft2)
1.89

2.10
1.87

1.95
1.89

1.98
2.06
1.88
1.86
1.89
1.89
1.89
1.89
1.89
3.21


3.96

2.05
2.05
1.70
1.70
0.88
1.07
3.10

1.48
-

2.32

Solids
Recovery
(%)
70.3

66.2
74.2

68.1
74.8

84.8
67.5
73.1
62.8
80.8
75.2
67.8
75.2
57.3
66.0


75.3

59.0
87.8
84.0
89.0
90.0
84.0
65.6

92.5
-

-

Run
Time
(hrs)
2.5

2.5
4.0

4.0
4.0

4.0
4.0
4.0
5.0
1.0
1,0
1.0
1.0
1.0
2.0


3.5

1.0
1.0
0.5
0.5
1.5
2.0
8.0

3.0
-

4.0

Screen
Type
(Mesh)
200

200
*

200
200

200
200
200
200
200
200
200
200
*
200


200

200
200
200
200
200
200
200

200
200

*

Comments
Solids recovery data obtained —
comp. force recorded.

Holes noticed in screen. New
screen 200.

Chem. feed pump malfunction —
comp. roller stalling.
Comp. roller stalling
Comp. roller again stalling.
Replaced chem. feed pump.





Changed screen after test runs-200.
Changed over to digested sludge —
using clips to fasten belt - pump
clogged.
Comp. roller stalling - poor cake
pick up.
Changed back to activated sludge.

Cake solids not measured.
Corap. roller stalling.
Sludge diluted by heavy rainfall.
Sludge diluted by heavy rainfall.
Changed to digested sludge — wait-
ing for normal RAS conditions.
Changed back to activated sludge.
Tried mixed primary - no data

Screen tore on cleaning — replaced
with 300 mesh.


-------
                           Table 3-B  Pilot Test Unit - Summary of Data From Oct.  11 through Nov.  16,
                                      1972 - Initial Study of Machine Parameters on Waste Activated  Sludge.
Run
1011
1012
1012-A
1016
L017-A
101 7-B
1017-C
1018

1027

1031
1031-A
1102
1106-A
1106-B
1106-C
1107-A
1107-B
1107-C
1110-A
1110-B
1113-A
1113-B
1114-A
1114-B
1116-A
1116-B


Sludge
Act
Act
Act
Act
Act
Act
Act
Act

Act

Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act


Coagulant
Type
C-31
C-31
C-31
C-31
C-31
C-31
C-31
C-31

None

C-31
C-31
C-31
C-31
C-31
C-31
None
C-31
C-31
C-31
C-31
None
C-31
C-31
C-31
None
C-31


(Ibs/
ton)
2.8
4.5
6.7
-
4.5
2.0
3.9
4.5

0

94.0
70.0
18.7
29.0
44.5
62.5
0
3.0
11.6
5.4
13.4
0
3.0
5.1
7.6
0
3.2


Cake
Solids
(%)
18.2
18.0
17.6
-
-
18.2
18.7
-

18.0

19.1
18.3
17.0
17.7
17.7
16.7
16.0
16.5
16.7
15.5
16.5
17.3
17.3
17.2
17.0
16.0
16.6


Comp.
Force
(Ibs/
in)
18.5
18.5
18.5
-
-
20.4
20.4
-

20.4

16.4
16.4
20.6
18.5
18.5
18.5
16.4
16.4
16.4
18.5
18.5
16.4
16.4
16.4
16.4
16.4
16.4


Solids
Loading
(Ibs/
ft2)
0.0071
0.0069
0.0069
-
0.0067
0.0067
0.0067
0.0213

0.0057

0.0054
0.0054
0.0042
0.0043
0.0043
0.0043
0.0031
0.0031
0.0031
0.0028
0.0028
0.0075
0.0075
0.0067
0.0067
0.0042
0.0042


Machine
Capacity
(Ibs/
hr ft2)
1.98
2.05
2.05
-
1.85
1.85
1.85
-

1.36

1.29
1.29
3.02
3.06
3.06
3.06
2.79
2.79
2.79
3.54
3.54
1.81
1.81
1.73
1.73
3.02
3.02


Solids
Recovery
(*)
88.0
82.0
83.0
-
-
83.0
90.0
-

74.0

99.5
99.1
91.1
88.0
85.5
91.0
59.0
75.9
94.0
77.0
84.0
69.4
68.0
75.0
85.0
51.1
60.3


Run
Time
(hrs)
4.0
4.0
1.0
3.5
1.0
1.0
1.0
1.0

1.5

2.0
1.5
2.0
1.0
1.0
1.0
1.0
1.5
0.5
2.5
2.5
1.0
1.0
1.0
1.0
1.0
1.0


Screen
Type
(Mesh)
300
300
300
300
300
300
300
300

300
*
200
300
300
300
300
300
300
300
300
300
300
300
300
300
300
300
*


Comments
Now using 300 mesh screen.


Lost data.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Capillary profile study. Screen
developing holes.
Screen tore. Changed screens for
next run .
New screen.


Problem w/sludge cake detachment.





Capillary profile study.
Capillary profile study.





Screen tore. Changed screens
after run.

 I
OS

-------
Table 4-B  Pilot Test Unit - Summary of Data From Dec. 1 through Jan.  1,
           1973 - Continue Study of Machine Performance on Waste Activated
           Sludge.
Run
1201-A

1201-B
1201-C
1201-D
1204-A
1204-B

1218-A
1218-B
1218-C
1219-A
1219-B
1219-C
1220-A
1220-B
1220-C
109 (73
117 (73
ludge
Act

Act
Act
Act
Act
Act

Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Act
Coagulant
Type
None

C-31
C-31
C-31
C-31
C-31

C-31
C-31
C-31
FeCl3
FeCl3
FeC 13
FeCl3
FeC IT
FeC IT
FeC 1^
FeCli
(Ibs/
ton)
0

8.2
5.6
2.6
18.5
11.7

55.0
41.0
12.0
57.6
34.6
23.0
542.0
401.0
293.0
209.0
127.0
Cake
Solids
(%)
14.5

14.1
14.5
15 ."5
14.5
16.1

15.5
15.8
-
13.1
15.0
13.7
16.3
18.3
14,3
15.0
15.2
Comp.
Force
(Ibs/
in)
12.4

12.4
12.4
12.4
12.4
12.4

12.4
12.4
-
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
Solids
Loading
(Ibs/
hr ft2)
0.0044

0.0044
0.0044
0.0044
0.0045
0.0045

0.0043
0.0043
0.0043
0.0042
0.0042
0.0042
0.0042
0.0042
0.0042
0.0042
0.0051
Machine
Capacity
(Ibs/
hr ftz)
4.6

4.6
4.6
4.6
4.6
4.6

4.5
4.5
4.5
4.3
4.3
4.3
4.3
4.3
4.3
4.3
5.3
Solids
Recovery
(%)
53.0

80.0
75.0
64.0
92.2
68.0

87.0
87.0
85.0
77.0
65.0
60.5
93.0
93.5
94.0
90.5
90.8
Run
Time
(hrs)
1.0

1.0
1.0
1.0
1.0
1.0

1.0
1.5
1.5
1.5
1.5
1.5
1.7
2.2
2.1
1.5
1.6
Screen
Type
(Mesh)
300

300
300
300
300
300

300*
300
300
300
300
300
300
300
300
325*
300
Comments
Using new screen. Running belt
at high speeds.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Shaft on drive roller broke.
Question solids recovery number.
New screen - same mesh
Capillary profile study.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Capillary profile study.
Screen tore-replaced w/325 mesh.
Capillary profile study.

-------
Table 5-B
Pilot Test Unit - Summary of Data From Jan. 26 through Feb.  14,
1973 - Continue of Study of Machine Performance with Digested
and Mixed Primary Sludges.



Run
126 (73)
129-A(73)
129-B
129-C
130-A(73)
130-B
131-A(73)
131-B
213-A(73)
213-B
213-C
21 3-D
214-A(73)
214-B
214-C



Sludge
Digst
Digst
Digst
Digst
Digst
Digst
Digst
Digst
Mix-Prim
Mix-Prim
Mix-Prim
Mix-Prim
Mix-Prim
Mix-Prim
Mix-Prim

Coagulant

Type
None
FeCl3
FeCl3
FeCl3
FeCl3
FeCl3
FeCl3
FeCl3
None
FeCl3
Fed 3
FeCl3
FeCl3
Fed 3
FeCl3
(Ibs/
ton)
0
43
73
14.2
170
242
345
460
0
17.5
52.6
89.4
172
246
369

Cake
Solids
a)
13.4
15.3
15.9
14.8
15.8
18.4
16.4
16.0
14.0
14.5
14.7
15.0
15.il
15.0
15.3
Comp.
Force
(Ibs/
in)
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
12.4
Solids
Loading
(Ibs/
ft*)
0.0056
0.0060
0.0060
0.0060
0.0050
0.0050
0.0053
0.0053
0.0056
0.0056
0.0056
0.0056
0.0060
0.0060
0.0060
Machine
Capacity
(Ibs/
hr ft2)
5.74
6.18
6.18
6.18
5.17
5.17
5.45
5.45
5.05
5.05
5.05
5.05
5.05
5.42
5.42

Solids
Recovery
(%)
55.3
65.2
71.7
61.3
81.0
88.4
92.4
97.3
56.8
59.5
67.0
74.6
80.5
84.3
84.9

Run
Time
(hrs)
2.0
1.5
1.5
1.5
2.0
2.0
2.0
2.0
1.5
1.5
0.5
1.5
1.5
1.5
2.0

S crccn
Type
(Mesh)
325*
325
325
325
325
325
325
325
325
325
325
325
325
325
325



Comments
New screen.















-------
                                 SECTION VIII

              APPENDIX C - Economics of Capillary Dewatering on
                           Waste Activated Sludge


Any product or process which is to be used by customers and for which there
are substitute products available must be economically justifiable in order
to be useful.  To this end, an estimate of the cost of dewatering waste activated
sludge by the capillary suction method must ultimately be considered.

The task of providing a detailed cost prediction for this process under all
possible operating conditions is extremely difficult because of the number of
parameters of choice which the customer can vary.  Since machine capacity and
performance is the ultimate design parameter which will set the equipment size,
the foremost question is under what conditions will the capacity be measured.
The parameters of choice are independent of each other over small ranges but
interdependent over gross ranges.   These include:
          •  Exit solids concentration
          •  Solids capture percentage
          •  Coagulant type (inorganic or polyelectrolyte)
          •  Feed solids concentration

In addition, dependent variables such as belt contact times and solids loading
rates have an effect on capacity also.  Earlier in this paper, curves were
presented showing the capacity as a function of polymer dosage and solids loading
rate.  If similar curves were available for feed solids concentration and solids
capture as functions of the other parameters, then an economic analysis could be
made that would be very inclusive.

To eliminate these problems and still provide a justifiable economic analysis,
cost estimates were made for three selected operating conditions which were
demonstrated during the course of the program.   The calculations assume a constant
machine size and an activated sludge of 2% as feed to facilitate run to run
comparisons.

Using these assumptions as a basis, sewage plant size will be a variable in the
comparisons.  Extension of the assumptions to larger scale plants such as 10 to
100 mgd would require substantiating the data at plant scale.

Costs were developed (Table C-l) at two levels of machine capacity i.e., 2.0 and
4.5 Ibs/hr ft  (10 and 22 Kg/hr m2) and for two coagulants at the higher capacity;
ferric chloride and a cationic polyelectrolyte.  The only costs considered are:

             machine capital
             maintenance and repair
             electrical
             coagulant
             labor
                                      - 66 -

-------
Costs such as building, land,  feed systems, removal systems, and ultimate
disposal were not considered due to the wide variations possible in these
systems and the fact that many of these facilities are available in existing
plants.  The costs shown in Table C-l are for the dewatering function only.

There are several interesting items to note in these costs.   As usual, the labor
costs are a significant portion (50% or more) of the cost of dewatering the
sludge.  The 1/2 man day estimate may be high since once the unit is started,
it should run automatically.  Because of the preparation and clean up time,
however, a half man day is probably realistic.

The coagulant costs for both ferric chloride and polyelectrolyte are similar
with a higher cost for the polymer.  The  ferric seemed to perform better but
has corrosion problems.  A cost of $3/ton ($3.30/metric ton) is not unreasonable
for this type of treatment however.

The power costs in this system are of note because they are so low.  At $130/year,
they are only 3% to 5% of comparable costs for centrifuges or vacuum filters.
With the cost of power increasing very rapidly, and present emphasis on energy
conservation, the low power cost makes this  method attractive.

                                                  22                 2
Decreasing machine capacity from 4.5 pounds/hr ft   (22 Kg/hr m )  to 2  Ibs/hr ft
(10 Kg/hr m^) essentially doubles  the  total  cost.  The machine capacity markedly
affects  the  system economics.  The exit  dry  solids in the lower  capacity  case
are significantly higher  than  the high capacity  case  which will  offset some of
the cost.  These figures point out the trade off  capability of  the system.

The costs detailed here  are competitive  with existing systems  such as  vacuum drum
filters, pressure filters,  and centrifuges.   In  fact, on waste activated sludge,
achievement  of  15%  to  17% solids  is  extremely difficult  with other systems.
                                   - 67 -

-------
                                  Table  1-C
                   Cost Estimates For Capillary Dewatertng
                          Basis for Cost Calculation
Assumptions
1.  Capillary device capital cost is $300 per active square foot of capacity and
    is linear with capacity.
                          2
2.  Machine size is 110 ft  of active areas.
3.  Operation schedule is 8 hour/day, 7 days/week, 360 days/year.
4.  Machine performance as in run 1218A data sheet.
    Performance data: 55 Ibs/ton ferric chloride as coagulant
                      4.5 Ibs/hr ft2 machine capacity
                      87% solids capture
                      15.5% exit solids cake
                      Waste activated sludge feed of ^2% solids
5.  No costs for overhead, peripheral feed equipment, or building.
Annual Cost Calculations
1.  Capital
    110 ft2 machine at $300/ft2 = $33,000
    Amortization over 20 years at 6%                      $2,877
    (m2 = .093 ft2, Kgs/ton(m) = 2.0 Ibs/ton, Kgs/m2 = 0.205 lbs/ft2,
            Kg = 2.2 Ibs, ton(m) = 1.1 ton, (HP- M  = .986 HP)
2.  Coagulant cost at 5c/lb ferric chloride
    4.5 Ibs   , in f2   8 hours    360 days     1 ton    _. „ rt
    - — x 110 ft  x — r -  x - *— x -nnA     = 712.8 tons
       .. 2                day       year      2000 Ibs
    hr r t
                                    3
                                    3
    (Approximately 4 mgd plant (16 m /day))
    712.8 tons x       _  x
                  ton       lb
3.   Power:  assume 5 hp  230 v 30 motor
    230v x 13a   3Kw
                    Shrs
           Kw-nr     day     year

                                   -  68 -

-------
                             Table 1-C (continued)



4.  Maintenance @ 5.5% of capital/year


    $33,000 x .055                                   $1,815



5.  Labor 1/2 man day/day at $5.QO/man hour



    4 man hours      $5       0,n  ,                   , onr.
    	 x 	Ir	  x 360 days                7,200
        day       man hour
Total annual cost for above items                   $13,804


Cost/ton = $13804/712.8                             $19.36/T
Run 12Q1B same conditions but polyelectrolyte


Performance data:  8.2 Ibs/ton C-31 polyelectrolyte as coagulant

                   4.6 Ibs/hr ft^ machine capacity

                   80% solids capture

                   14.1% exit solids cake

                   Waste activated sludge feed of ^2% solids



1.  Capital                                          $2,877



2.  Coagulant cost at 40c/lb C-31


    4.6 Ibs   1in ft_2   8 hrs   360 days     1 ton
    	 n  x 110 ft  x ——— x 	J— x n--- ..,— = 729 tons
    hr ft*               day     year      2000 Ibs


    (approximately 4 mgd plant (16 nH/day))


    -no        8.2 Ibs    $.40                        ^  .
    729 tons x 	x  y     =                     $2,391
                  ton      Ib


3,  Power                                            $   130



4.  Maintenance                                      $1,815



5.  Labor                                            $7,200
                                                     $14,413


 Cost/ton  =  $14,413/729                               $19.77/ton





 Run  1012A


 Performance data:   6.7  Ibs/ton C-31 polyelectrolyte coagulant

                    2.05 Ibs/hr ft2  machine capacity

                    83%  solids capture

                    17.6% exit solids cake

                    Waste activated  sludge feed at ^2% solids
                                  -69-

-------
                             Table 1-C (continued)

 1.   Capital                                         $2jg77
 2.   Coagulant cost at 40  870
3.   Power                                            $
4.   Maintenance                                      $1
5.  Labor                                            $7,200
                                                    $12,892
Cost/ton = 12892/325                                $39.67/ton
                                      - 70 -

-------
                                    TECHNICAL REPORT DATA
                             (Please read Instructions on the reverse before completing)
 1. REPORT NO.

   EPA 670/2-74-017
                                                            3. RECIPIENT'S ACCESSION-NO.
 4. TITLE AND SUBTITLE
   EVALUATION AND DEMONSTRATION OF THE CAPILLARY
   SUCTION SLUDGE DEWATERING DEVICE
                                          5. REPORT DATE
                                             March
                                          6. PERFORMING ORGANIZATION CODE
 7. AUTHOR(S)

   T. E. Lippert and M.  C.  Skriba
                                                            8. PERFORMING ORGANIZATION REPORT NO
 9. PERFORMING ORGMMIZATION NAME AND ADDRESS

   Westinghouse Electric  Corporation
   Research and Development Center
   Pittsburgh, Pennsylvania  15235
                                          10. PROGRAM ELEMENT NO.

                                             132043 -RQAP 21-ASP Task 09
                                          11. CONTRACT/GRANT NO.


                                             68-01-009^
 12. SPONSORING AGENCY NAME AND ADDRESS
   Office of Research  and Development
   National Environmental Research Center
   Environmental Protection Agency
   Cincinnati. Ohio  4*5268
                                          13. TYPE OF REPORT AND PERIOD COVERED
                                             Final report
                                          14. SPONSORING AGENCY CODE
 15. SUPPLEMENTARY NOTES
 16. ABSTRACT
   A device for dewatering waste activated  sludge that uses the capillary suction in
   a porous belt has been demonstrated on a pilot scale test unit.  The  system uses
   capillary action to  initially dewater the  sludge and form a thin sludge cake which
   is then mechanically compressed in a final step to obtain a still dryer cake.  Both
   dewatering steps are incorporated into a single system endless belt design.   Sludge
   feed capacities from 2 to 4.5 Ibs/hr ft2 (10  to 22 Kgs/hr m*) have been demonstrated
   with the cake solids at discharge ranging  from 15 to 18 percent.  These results were
   obtained with a conditioned waste activated sludge at a coagulant cost of approxi-
   mately $4.00/ton ($4.4o/metric ton).  The  device has also been tested on an
   anaerobically digested and a mixed primary-activated sludge.
                                KEY WORDS AND DOCUMENT ANALYSIS
                                                                        Jc. COSATI Field/Group
DESCRIPTORS
                            b.lD!
 *Sludge, «Sewage, Sludge Drying,  Cakes,
 Filtration, *Sludge treatment.  Deposition,
 Force,  Conditioning (treating)
 8. DISTRIBUTION STA I bMbN I

   Release to public

i
EPA Form 2220-1 (9-73)
                            *5iu
-------