EPA-650/2-75-025
March 1975
Environmental  Protection Technology  Series
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                                                         "•"•"•*•*•*•*•"•
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                               EPA-650/2-75-025
   METHODOLOGY FOR ASSIGNMENT
OF A  HYDROCARBON  PHOTOCHEMICAL
   REACTIVITY  INDEX FOR EMISSIONS
         FROM  MOBILE  SOURCES
                      by
        Francis M. Black, Larry E. High, and John E. Sigsby
             Chemistry and Physics Laboratory
                  ROAP No. 26ACV
               Program Element No. 1AA010
           National Environmental Research Center
            Office of Research and Development
            U.S. Environmental Protection Agency
         Research Triangle Park, North Carolina 27711

                   March 1975

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                        EPA REVIEW NOTICE

This report has been reviewed by the National Environmental Research
Center - Research Triangle Park, Office of Research and Development,
EPA, and approved for publication.  Approval does not signify that the
contents necessarily reflect the views and policies of the Environmental
Protection Agency, nor does mention of trade names or commercial
products constitute endorsement or recommendation for use.
                    RESEARCH REPORTING SERIES

Research reports of the Office of Research and Development, U.S. Environ-
mental Protection Agency, have'been grouped into series.  These broad
categories were established to facilitate further development and applica-
tion of environmental technology.  Elimination of traditional grouping was
consciously planned  to foster technology transfer and maximum interface
in related fields.  These series are:

          1.  ENVIRONMENTAL HEALTH EFFECTS RESEARCH

          2.  ENVIRONMENTAL PROTECTION TECHNOLOGY

          3.  ECOLOGICAL RESEARCH

          4.  ENVIRONMENTAL MONITORING

          5.  SOC1OECONOMIC ENVIRONMENTAL STUDIES

          6.  SCIENTIFIC AND TECHNICAL ASSESSMENT REPORTS

          9.  MISCELLANEOUS

This report has been assigned to the ENVIRONMENTAL PROTECTION
TECHNOLOGY series. This series describes research performed to
develop and demonstrate instrumentation, equipment and methodology
to repair or prevent  environmental degradation from point and non-
point sources of pollution.  This work provides  the new or improved
technology required for the control and treatment of pollution sources
to meet environmental quality standards.
This document is available to the public for sale through the National
Technical Information Service, Springfield, Virginia 22161.

                 Publication No. EPA-650/2-75-025
                                 11

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                              CONTENTS
                                                            Page
LIST OF FIGURES	     iv



LIST OF TABLES	     iv



ACKNOWLEDGMENTS 	     iv



INTRODUCTION  	      1



EXPERIMENTAL  	      3



RESULTS AND DISCUSSION  	     13



CONCLUSIONS   	     21



REFERENCES	     22



TECHNICAL REPORT DATA AND ABSTRACT  	     23
                                  iii

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                            LIST OF FIGURES


Figure                                                          Page


  1                  Gas Chromatographic System Block  Diagram       4

  2                 Chromatographic Flow Scheme                   5

  3                 System Operation  Sequence                     7

  4                 Chromatogram of Calibration Mix               9

  5                 Valve Programmer                              11

  6                 Exhaust Chromatogram, Catalytic Effect         20
                            LIST OF TABLES


Table                                                            Page


  1                 Reactivity Classification of Mobile             2
                    Source Hydrocarbon Emissions

  2                 Hydrocarbon Reactivity Class Average          15
                    Carbon Numbers, Fuel

  3                 Hydrocarbon Reactivity Class Average          16
                    Carbon Number, Exhaust

  4                 Photochemical Significance of Hydro-          18
                    carbon Emissions from Light-Duty
                    Mobile Sources
                           ACKNOWLEDGMENTS

     We would  like  to acknowledge and give special recognition to the
Emissions Testing and Characterization Section of the Chemistry and
Physics Laboratory, particularly Dr. R. Bradow and Mr. F. King, for
their efforts  in providing the mobile source exhaust samples utilized
in this work.
                                   iv

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              METHODOLOGY  FOR  ASSIGNMENT
  OF A  HYDROCARBON  PHOTOCHEMICAL  REACTIVITY  INDEX
           FOR EMISSIONS FROM  MOBILE  SOURCES
                          INTRODUCTION
     Air quality criteria for photochemical oxidants have been established
in accordance with Section 107(6)  of the Clean Air Act (42 U.S.C.
1857-18571).   The current approach to abatement of photochemical  oxidants
is based on control  of organic emissions.  Mobile source certification
procedures dictate control of total hydrocarbon emissions.  Many studies
                 2-5
have been reported   that indicate that organic emissions participate in
atmospheric reactions leading to oxidant/ozone formation in varying degrees,
The consensus of these studies indicates that methane, ethane, acetylene,
propane, and benzene, under reasonable hydrocarbon-to-NO  ratios,  are
                                                    /\
essentially nonreactive.
     Since the standard requiring hydrocarbon emission control is  based on
oxidant/ozone formation, procedures for measurement of both mass and reac-
tivity of hydrocarbon emissions are necessary to evaluate adequately the
potential impact on photochemical  pollution of prototype hydrocarbon con-
trol systems.
                               1

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     Current research practices entail detailed analysis of more than 50
hydrocarbon compounds commonly found in exhaust samples.  These are
weighted by reactivity.  The chromatographic procedures required for the
analysis of the individual hydrocarbons are cumbersome and beyond the
capabilities of many interested laboratories.  It is the intent of this
report to suggest less cumbersome procedures that will permit assignment
of a  Hydrocarbon Photochemical Reactivity Index  for mobile sources.
     Hydrocarbon reactivity has been utilized as an index of participation
in atmospheric reactions leading to oxidant/ozone formation.  Within the
context of this report, hydrocarbons will be addressed in four basic
reactivity classes as set forth in Table 1.
          Table  1.   REACTIVITY  CLASSIFICATION OF MOBILE  SOURCE
                         HYDROCARBON  EMISSIONS5
Class
I (nonreactive)
II (reactive)
III (reactive)
IV (reactive)
Compounds
Methane, ethane,
acetylene, propane,
benzene
C^ and higher paraffins
Aromatics less benzene
Olefins
Molar
reactivity rating
1.0
6.5
9.7
14.3
     A  newly  developed gas  chromatographic  procedure  for measurement of
 the  nonreactive  hydrocarbons,  Class  I, will  be  discussed in  detail.  Fur-
 ther, the  integration  of this  procedure with previously described  sub-
 tractive techniques  will be discussed for  measurement of  the  three
 reactive classes.

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                            EXPERIMENTAL
NONREACTIVE  HYDROCARBON MEASUREMENT
     A gas chromatographic system has  been developed  that will  permit
quantitative analysis of methane, ethane,  acetylene,  propane, and  benzene.
The system,  which includes four packed columns  operated  in  a  Perkin-Elmer
Model 900 gas chromatograph (GC) equipped  with  a flame ionization  detector,
is basically illustrated in Figure 1.   Multiple columns  are required
because of the significantly different physical and chemical  character  of
the compounds being determined and because of the large  variety of poten-
tially interfering compounds found in normal  samples. The  interfering
compounds include a wide range of other hydrocarbons, oxygenates,  sulfur-
and nitrogen-containing organics, and the  inorganics  0»» N^,  CO^,  CO,  NO,
and N0«.  The described column system permits baseline resolution  of  the
five hydrocarbons defined as nonreactive.
     The method involves injection of two  sample aliquots:  The first  on
columns 1 and 2 for methane, ethane, acetylene, and propane analysis;  and
the second on columns 3 and 4 for benzene  analysis.  Both aliquots are
directed to a single detector, with columns 1 and 2 being backflushed  to
vent during the period when benzene is eluting from columns 3 and  4.   The
second aliquot is injected so as to permit elution of the C«  hydrocarbons
of interest prior to elution of the benzene.
     The details of the system are illustrated in Figure 2.  Column 1,
which consists of 96- by 1/8-inch o.d. stainless steel tube packed with
80/100-mesh Poropak Q, is used primarily to resolve methane from air.
Normally, air is considered not to produce a signal of significance in
a  flame ionization detector.  However, when the detector/signal amplifier

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                             CARRIER
                               GAS
SAMPLE
 INLET '




SAMPLE
VALVE
1
u
SAMPLE
LOOP I




ANALYTICAL
COLUMNS
1AND2


VENT \






VENT

SAMPLE I
LOOP
O


VENT f


SAMPLE
WAI V/C
VALVt
2


VENT


ANALYTICAL
pni IIMUC
COLUMN?
3 AND 4







nFTFrrnn SIGNAL
DLTCCTOR PROCESSOR






                             CARRIER
                               GAS
                                   Figure 1.  Gas chromatographic system block diagram.

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                                                                    NOTE:
CJl
          PRESS. REG.

       PRESS. GAUGE

           NEEDLE
            VALVE
              FLOW   -|
           CONTROLLER

                  *
A, B, C, D, J      SIX-PORT SEIZCOR GAS-SAMPLING VALVES

E, F, G, H       THREE-WAY SOLENOID VALVES

              CHROMATOGRAPHIC ANALYTICAL COLUMNS

              RESTRICTED 0.01 x 6-inch CAPILLARY
                                                     SO psig
              rAiR       *                        mnm
                    SAMPLE INLET
                                                  Figure 2. Chromatographic flow scheme.

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is operated with sensitivity appropriate to methane levels in samples from
emission-controlled vehicles, the signal resultant from the oxygen in air
is significant and must be resolved from methane.  Although the flame
detector responds only to hydrogen-carbon compounds, when the air peak
enters the detector it momentarily changes the ionization characteristics
of the flame and interplays with the background hydrocarbon signal to
yield a positive system response.  On the system described, this signal
is equivalent to 0.9 part per million carbon (ppm C).  Column 2 consists
of a 48- by 1/8-inch o.d. Teflon tube packed with 35/60-mesh Type 58
Silica Gel and is used to resolve the Cp and C3 hydrocarbons.
     Column 3 consists of a 180- by 1/8-inch o.d. stainless steel tube
packed with 15 percent 1,2,3-tris (2-cyanoethoxy) propane on acid-washed
60/80-mesh firebrick and is used to resolve benzene from the other aro-
                                                 o
matics and from the paraffins/olefins/acetylenes.   Column 4 consists of a
24- by 1/8-inch o.d. stainless steel tube packed with 20 percent HgSO. on
30/40-mesh firebrick and is used to resolve benzene from the oxygenated
hydrocarbons.  The firebrick columns were prepared utilizing acetone and
water solvents for columns 3 and 4, respectively.  The substrates used for
the preparation of columns 3 and 4 were conditioned in a vacuum oven at
110°C for 24 hours prior to column packing.
     The stainless steel columns are 0.093-inch i.d., and the Teflon col-
umn is 0.0625-inch i.d.; all are operated with a helium carrier at 50
cm /minute.
     Figure 3 illustrates the analytical sequence on a time-temperature
plot appropriate to the system described.  The temperature program indi-
cated applies only to columns 1 and 3.  Columns 2 and 4 are maintained

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o
o
     60 	
     50
     40
                                     GC OVEN TEMPERATURE
                                                                         STEP
                                                                          5
     30
                                                        I       I   /  I
                                            STEP
                                              6
       0       1
11       12       13       14       15       16       17  ' '   26      27      28
                                                               TIME, minutes
                                               Figure 3. System operation sequence.

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isothermal at room temperature (20°C).  In the time-zero configuration,
sample valves A and B are ready for loading, columns 1 and 2 are fore-
flushing to the detector, column 3 is foreflushing to the vent, and column
4 is backflushing to the vent.  The analytical sequence includes loading
                                3
sample valves A and B with 10-cm  sample aliquots and the following
steps, as illustrated in Figure 3:
     Step 1.  Inject sample aliquot A on columns 1 and 2 for C,
                                                              i >
              C2> and Co analysis and begin 35°C isothermal GC oven
              operation.
     Step 2.  Begin GC oven temperature elevation from 35°C to
              100°C at 32°C/minute.
     Step 3.  Inject sample aliquot B on column 3 for benzene
              analysis.
     Step 4.  Begin 100°C isothermal GC oven operation.
     Step 5.  Simultaneously switch valves C and J, directing
              the flow in columns 1 and 2 to the backflush vent,
              and directing the flow in column 3 through column 4
              to the detector.
     Step 6.  Switch valve D directing flow in column 3 to the
              backflush vent.
     Step 7.  Reset all valves to time-zero configuration, and
              lower GC oven temperature to 35°C.
     Figure 4 illustrates the resultant chromatogram.
     To facilitate reproducible valve sequencing, a programmer utilizing
three timers (Automatic Timing and Controls, Inc.) has been designed that
permits manual and automatic cycling of the valves.  The programmer is
                                  8

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METHANE
  AIR
          i        i        r
ETHYLENE
r
                    i       i        r
                                   ETHANE
                                   ACETYLENE
                  I       I        I
i        i        r
                                                                    PROPANE
                                                                               PROPYLENE
                                                                                                      BENZENE
                                  56789




                                          RETENTION TIME, minutes




                               Figure 4.  Chromatogram of calibration mix.
                                                     10
                                                     11
                12
13
14

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illustrated in Figure 5.  Valves A, B, C, D,  and J are actuated  with  high-
pressure air (50 psig) controlled by solenoid valves E, F,  G,  and H inter-
faced to the programmer.  To determine the appropriate valve sequencing,
the programmer is operated in the manual  mode.  Utilizing a calibration
mix including methane, ethane, ethylene,  acetylene, propane, propylene,
and benzene, sample aliquot A is injected on  column 1.  The GC oven is
maintained at 35°C until after air and methane have eluted.  The oven
temperature is then rapidly elevated to 100°C.  The rate at which the
temperature is elevated is determined by the  C^ and C~ hydrocarbon reso-
lution.  With the time of Steps 1, 2, and 4 established, Step 5 is deter-
mined by the elution of propylene.  The time  at which sample aliquot B  is
injected is determined by the elution time of benzene from column 3 in
relation to the time of Step 5.  This can be  observed by manually setting
columns 1 and 2 to backflush through the vent and directing the flow of
columns 3 and 4 to the detector, and then injecting sample aliquot B.
The paraffinic/olefinic/acetylenic compounds  will elute 2 to 6 minutes
after injection, and the benzene elutes about 10 minutes after injection.
Step 3 is executed so as to permit elution of propylene, switching the
columns to the detector (Step 5), and establishing baseline prior to
elution of benzene.  Step 6 is executed after completion of the benzene
elution, and Step 7 is performed after column 3 has backflushed for a
period equivalent to the period running from injection of aliquot B to  the
benzene elution.  The three ATC timers are set using the time of Step 3
for timer I, the time of Step 5 for timer II, and the time of Step 6 for
timer III.  The programmer can then be utilized in the automatic mode
for reproducible sequencing.
                                    10

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TIMER
  I
TIMER
                             •1
                             .2
                              3
                           r-4
                              9—J
                           ^-11
                              12 —
                           — 14
                              15  —J
                                                                  SAMPLE
                                                                   PUMP
                                                           SOL "E
1 1
1
1

SOL '
^
' 1
1
| NOTE:
TIMER
  III
                          TIMER: ATC MODEL 325A346 A10PX
                          SI:  DOUBLE POLE, DOUBLE-THROW SWITCH
                          S2-6: SINGLE POLE, SINGLE-THROW SWITCH
                          Rl-3: RELAY
                          SOL: SOLENOID VALVE
                          L: LIGHT
                          F: FUSE
Figures.  Valve programmer.

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     A Perkin-Elmer Model PEP-1 Data Processor is utilized with the system
to facilitate rapid transposition of peak data to concentration.  The
processor is utilized with a calibration mix to compute response factors
for each compound.  The response factors are stored with peak retention
data permitting on-line reporting of each sample compound by name and
concentration.  System analytical repeatability is + 1.5 percent.
REACTIVE HYDROCARBON MEASUREMENT
     As indicated in Table 1, there are three classes of reactive hydro-
carbons of interest:  C^ and higher paraffins, aromatics except benzene,
and olefins.  Three participant components of this definition can be
obtained using the subtractive techniques of Klosterman:  total hydro-
carbon (THC) level, paraffin plus aromatic (PA) level, and paraffin plus
benzene (PB) level.  The procedures for obtaining these values are well
described and will not be discussed further.  Reactive class values can be
obtained by the following methods:  (1) for class II by subtracting the
sum methane + ethane + propane + benzene from (PB); (2) for class III by
subtracting (PB) from (PA); and for class IV by subtracting (PA) +
acetylene from (THC).
     Reactive hydrocarbon measurement may be summarized for the classes
by the following equations:
     Class I   = methane + ethane + propane + acetylene + benzene
     Class II  = (PB) - (benzene + methane + ethane + propane)
     Class III = (PA) - (PB)
     Class IV  = (THC) - (PA + acetylane)
                                   12

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                        RESULTS AND DISCUSSION
     Currently defined procedures  for certification of  light-duty motor
        g
vehicles  call for collection  of three  exhaust  samples:   sample  1,
"transient cold start" test-phase  emissions;  sample 2,  "stabilized cold
start" test-phase emissions; and sample 3,  "transient hot start" test-
phase emissions.  These samples are  collected with a Constant  Volume
Sampler, which dilutes the auto exhaust with  air.  Three  dilution air
samples are collected concurrent with the exhaust samples.  There are
thus six hydrocarbon analyses  required  per  certification  run—three
samples and three backgrounds.  These values  are utilized to calculate
the weighted mass emissions of hydrocarbons in  grams per  vehicle mile.
The suggested procedure inserts reactivity  in this calculation and
results in a Hydrocarbon Photochemical  Reactivity Index for the  vehicle.
CALCULATIONS
     The reactivity rating for each  test-phase  sample is  calculated as
follows:
                (% I x r^ + (% II x r2) +  (% III x r3) + (%  IV  x r4)   (5)
     Rht,s,ct =                          TOO
     where:
            R  = reactivity rating value calculated for each  test phase,
                 i.e., cold transient,  stabilized, and  hot transient.
     % I, II, III, IV = mass percentage of  total hydrocarbon  determined
                        to be  in  classes I, II, III, and  IV,  respectively.
                                 13

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          « T  =100 exhaust class I hydrocarbons, ppm C
                     exhaust total hydrocarbons, ppm C
     rl 2 3 4  = mass reactiv1ty rating for class I, II, III. and IV
                 hydrocarbons.
     A prerequisite for the determination of class mass reactivity ratings
is definition of the average carbon number of the class emissions.  The
average carbon number can be used in conjunction with the molar reactivity
ratings given in Table 1 to determine the mass reactivity ratings.
Detailed hydrocarbon analysis is required to determine the class average
carbon number.  The procedures described generate a detailed analysis of
class  I, but not of classes II, III, and IV hydrocarbons.  Tables 2 and 3
tabulate class average carbon numbers for several fuels and exhaust samples,
respectively, as determined by detailed hydrocarbon analysis.
     As can be seen, the average carbon number is dependent on fuel and on
the combustion/control system.  The sampling procedures (test cycle) will
also affect the exhaust class average carbon number.
     The reactivity ratings utilized by the author will be based on samples
resultant from vehicles operated with the current Federal Test Procedure
(three test phases) and a regular-grade unleaded fuel.  The average carbon
numbers utilized to determine the mass reactivity ratings are 5.55, 7.58,
and 2.85 for classes II, III, and IV, respectively.  Class I ratings are
determined on a sample-by-sample basis as detailed information is available.
               -  =
                    _   _
                1   average carbon number of test phase
                    class  I hydrocarbons
           r        6.5, 9.7  , 14.3
            2,3,4   5.5  7.58  2758
           r      = 1.2,  1.3, 5.0
            2,3,4
                                  14

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               Table 2.   HYDROCARBON REACTIVITY CLASS
                    AVERAGE CARBON NUMBERS,  FUEL
Sample
Fuel (1)
API-1
Premium leaded
1968
Fuel (2)
API -8
Premium unleaded
1968
Fuel (3)
API-10
Regular unleaded
1968
Fuel (4)
Indolene
Regular unleaded
1972
Fuel (5)
Phillip's 66
EPA special
Regular unleaded
1973
Average carbon number,
reactivity class
I
6.00
6.00
6.00
6.00
6.00
II
6.18
5.78
5.72
6.31
6.68
III
7.43
7.85
7.99
7.49
7.63
IV
6.08
5.59
5.91
4.67
4.87
     As specified in the Federal  Register.9 the mass emissions for each
test phase are calculated as follows:
                 = V mix x density HC x
                                        HC  onc
     where:
               Y = mass emissions in grams hydrocarbon per test phase
           V mix = total  dilute exhaust volume in cubic feet per test
                   phase corrected to standard conditions (528°R and
                   760 mm Hg).
                               15

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           Table 3.  HYDROCARBON REACTIVITY CLASS
              AVERAGE CARBON NUMBERS, EXHAUST
Sample
1968 vehicle
1969 Federal Test
Procedure
Fuel (1)
1968 vehicle
1969 Federal Test
Procedure
Fuel (2)
1968 vehicle
1969 Federal Test
Procedure
Fuel (3)
1972 Chevrolet
1972 Federal Test
Procedure
Fuel (5)
1975 prototype "A"
1972 Federal Test
Procedure
Fuel (5)
1975 prototype "B"
1972 Federal Test
Procedure
Fuel (5)
i
Test
phase











•
I
II
III

I
II
III

I
II
III

Average carbon number,
1 reactivity class
I
1.58



1.77



1.76


f
1.52
1.44
1.58

1.46
1.04
1.22

1.37
1.02
1.15

II
6.35



5.97



5.88



5.85
5.51
5.79

5.37
5.43
5.14

5.93
5.44
5.49

III
7.55



7.98



8.07



7.40
7.43
7.40

7.57
8.29
7.62

7.39
7.80
7.34

IV
3.16



3.54



3.36



2.72
2.56
2.66

3.01
2.78
3.54

2.72
2.87
2.80

Density HC = density of hydrocarbons in the exhuast gas
             assuming an average carbon-to-hydrogen ratio
             of 1:1.85 in grams per cubic foot at 528°R
             and 760 mm Hg pressure (16.33 g/ft3).
             (Note:  Current EPA policy is to express all
             measurements in Agency documents in metric
             units.  When implementing this practice will
                            16

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                   result in  undue  difficulty in  clarity,
                   NERC/RTP is providing  conversion factors  for
                   the particular nonmetric units used in  the
                   document:   cubic foot  = 0.02832 cubic meter.)
         HC cone = hydrocarbon concentration of the dilute exhaust
                   sample corrected for background, in ppm carbon
                   equivalent.

     The Hydrocarbon Photochemical  Reactivity Index combines the  reactivity
rating with the mass emission of each test phase  and weights the  test
phases appropriately.
          (0.43 x Y   x R  )  + (0.57 x Y.   x RhJ + (Y  x  R )         (7)
   HPRI	—	—	775	—	—
APPLICATION
     As illustrated in Figure 4, in addition to the five nonreactive hydro-
carbons, definition of ethylene and propylene is  obtained  from the chroma-
tographic system.  Although the analysis  of these compounds is not used in
the scheme described, the compounds are relatively abundant in auto exhaust
samples and serve as excellent system check peaks.  They allow the operator
to ensure that the chromatographic carrier gas system is stable.   They also
account for a major portion of the difference between the  fuel and exhaust
olefin average carbon number.
     The purpose of the defined scheme is to permit relating the  various
hydrocarbon emission control  systems to the photochemical  significance of
the hydrocarbons being emitted.  To illustrate this application,  Federal
certification runs were conducted with a  variety  of vehicles as indicated
in Table 4.
                                                                    «
                                  17

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           Table 4.  PHOTOCHEMICAL  SIGNIFICANCE  OF 'HYDROCARBON EMISSIONS FROM LIGHT-DUTY MOBILE SOURCES



Vehicle
description
1972 Chevrolet


1975 prototype
"A" with
catalyst
removed
1975 prototype
"A" with
n Ti 1 Lit
catalyst
1n place
1975 prototype
11 B" with
catalyst
in place




Test phase
Cold transient
Stabilized
Hot transient
Cold transient
Stabilized
Hot transient
Cold transient

Stabilized
Hot transient
Cold transient
Stabilized
Hot transient
Reactivity class
I

Nonreactive,
percent
23.9
27.4
18.3
16.3
24.0
13.9
6.8

40.7
14.4
16.4
38.1
27.0
II
Reactive
paraffins,
percent
32.2
28.9
39.1
39.2
40.3
53.4
54.4

23.6
61.0
38.4
42.0
48.5
III
Reactive
aroma tics,
percent
20.6
18.3
21.0
24.3
15.2
16.7
10.0

21.4
8.4
22.9
8.2
11.5
IV
Reactive
olefins,
percent
23.4
25.3
21.6
20.2
20.6
16.0
28.8

14.3
16.2
22.2
11.7
13.0




R
1.98
2.04
1.93
1.91
1.91
1.75
2.27

1.55
1.77
1.99
1.57
1.62



V mix,
ft3
2955
5102
2997
2932
5168
3029
2964

5123
3012
2952
5097
2995



HC cone.,
ppm C
157.9
52.7
87.9
138.7
27.4
117.3
51.8

8.4
60.6
86.8
9.3
24.8




Y
7.62
4.39
4.79
6.64
2.31
5.80
2.51

0.70
2.98
4.18
0.77
1.21




HPRI

2.76


2.08



0.88


0.79

00

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     Prototype "A" gave a 66 percent improvement in mass emissions  rela-
tive to the 1972 Chevrolet; prototype "B" showed a 69 percent improvement.
Prototype "A" also gave a 12 percent improvement in the net reactivity
of the emissions, and prototype "B" showed a 16 percent improvement.   As
illustrated by the data in Table 4, catalytic emission control  systems
yield definite mass improvement but also reactivity improvement.   The
degree of mass and reactivity improvement varies between control  systems.
     The impact of catalytic control systems on individual  hydrocarbons,
resultant in the variable reactivity gains, is illustrated  in Figure  6.
As evidenced, the degree of control of the hydrocarbons is  variable with
individual hydrocarbons.  When the catalytic muffler was placed in the
appropriate position in the exhaust stream, the methane level was reduced
13 percent, whereas the acetylene was reduced 92 percent, the ethylene
74 percent, and the propylene 83 percent.
     An additional compound that may be observed on the chromatographic
system when utilized with vehicles without advanced emission control  is
propadiene.  The compound is baseline-resolved with a retention time  of
about 11.9 minutes, eluting after propylene.
                                 19

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 AIR
      7.7 ppm C
      METHANE
                                                    1975 PROTOTYPE "A"
                                                    CATALYST REMOVED
                        7.7 ppm C
                       ETHYLENE
                             6.1 ppm C
                            ACETYLENE
                                                                 5.8 ppm C
                                                                PROPYLENE
                                                                                2 J ppm C
                                                                               BENZENE
AIR
      6.7 ppm C
      METHANE
                                                    1975 PROTOTYPE "A"
                                                    CATALYST IN PLACE
                        2.0 ppm C
                       ETHYLENE
0.4 ppm C
ETHANE
 0.5 ppm C
ACETYLENE
                                                               1 0 ppm  C
                                                               PROPYLENE
                             1.4 ppm C
                              BENZENE
      I	I
 I      I      I      I
                I
I
                              6789

                              RETENTION TIME, minutes
                                     10
                                   11     12
                        13
14
             Figure 6.  Exhaust chromatogram. catalytic effect.
                                     20

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                               CONCLUSIONS
     The control of hydrocarbon emissions is necessitated by air quality
criteria for photochemical  oxidants.   In view of the fact that hydro-
carbons do not participate to the same extent in atmospheric reactions
leading to oxidant formation, methods for measurement of more than mass
of emissions are necessary to project adequately the impact of mobile
sources on photochemical  pollution.
     Hydrocarbon photochemical reactivity can be integrated with mass
measurement methods in varying degrees; total hydrocarbon mass emissions
can be measured with no assessment of atmospheric reactivity.  Total  hydro-
carbon less methane levels can be measured, eliminating the most abundant
nonreactive hydrocarbons.  Total hydrocarbon less methane, ethane, propane,
acetylene, and benzene levels can be measured, eliminating the essentially
nonreactive hydrocarbons.  The emissions can be measured in four hydro-
carbon classes, weighting by class reactivity.  The emissions can be
measured in detail, weighting each individual hydrocarbon by its atmos-
pheric reactivity.  Methodology permitting assessment in the first four
degrees is available by techniques discussed in this paper.  Although only
detailed analysis will result in absolute assessment, the procedures
described offer a very good approximation of the hydrocarbon photochemical
reactivity.  The technique is weakened only by the need to estimate class
average carbon number.  With definition of fuel and vehicle configuration,
this estimation can be made relatively accurately.
                                  21

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                              REFERENCES


1.   Air Quality Criteria for Photochemical  Oxidants.   U.S.  DHEW,  PHS,
     NAPCA, Washington, D.C., AP-63, 1970.

2.   Altshuller, A. P. and J. J. Bufalini.   Photochemical  Aspects  of
     Air Pollution:  A Review.  Environ. Sci.  Technol.  5_:   39-63,  1971.

3.   Altshuller, A. P., S. L. Kopczynski, D. Wilson,  and W.  A.  Lonneman.
     Photochemical Reactivities of N-Butane and Other Paraffinic Hydro-
     carbons.  J. Air Poll.  Cont. Assoc. J£:   787, 1969.

4.   Tuesday, C. S. and W. A. Glasson.  Hydrocarbon Reactivity  in  the
     Atmospheric Photooxidation of Nitric Oxide.  (Presented at ACS
     Meeting, Atlantic City, September 1965.)

5.   Dimitriades, B.  The Concept of Reactivity and Its Possible Appli-
     cation in Control.  In:  Proceedings of the Solvent Reactivity
     Conference.  U.S. Environmental Protection Agency, Research Triangle
     Park, N.C. EPA-650/3-74-010, November 1974.

6.   Klosterman, D. L. and J. E. Sigsby.  Application of Subtract!ve
     Techniques to the Analysis of Automotive Exhaust.   Environ. Sci.
     Technol. 1:  309-314, 1967.

7.   Bellar, T. A. and J. E. Sigsby.  Evaluation of Various  Silica Gels
     in the Gas Chromatographic Analysis of Light Hydrocarbons. Environ.
     Sci. Technol.  1:  242-246, 1967.

8.   Clemans, C. A., P. W. Leach, and A. P. Altshuller.  1,2,3-Tris
     (2-cyanoethoxy) Propane as a Stationary Phase in the Gas Chromato-
     graphic Analysis of Aromatic Hydrocarbons.  Anal.  Chem. 35:
     1546-1548, 1963.

9.   Title 40 - Protection of the Environment.  Part 85, Subpart A,
     Emission Regulations for New Gasoline-Fueled Light-duty Vehicles.
     Federal Register.  3_7(221):  24270-24277, November 1972.
                                  22

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                                TECHNICAL REPORT DATA
                         (Please read Instructions on the reverse before completing)
1  RLPORTNO
4 riTLI. ANUSUUTITLE
  Methodology  for  Assignment of  a Hydrocarbon
  Photochemical Reactivity Index for Emissions
  from Mobile  Sources ___
7 AUTHOR(S)
  F.  M.  Black,  L.  E.  High,  and J.  E.  Sigsby
                                                      3 RECIPIENT'S ACCESSION-NO.
            5 REPORT DATE
              March 1975
            6 PERFORMING ORGANIZATION CODE
                                                      8 PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORG \NIZATION NAME AND ADDRESS
  U.S.  Environmental  Protection  Agency
   National Environmental  Research Center
   Research Triangle Park,  N.C.  27711
            10. PROGRAM ELEMENT NO.
            1AAOIO.ROAP No. 26ACV
            11 CONTRACT/GRANT NO
12 SPONSORING AGENCY NAME AND ADDRESS
                                                       13. TYPE OF REPORT AND PERIOD COVERED
   National Environmental  Research Center
   Chemistry and  Physics Laboratory
   Research  Triangle Park,  N.C.  27711
            14. SPONSORING AGENCY CODE
15 SUPPLEMENTARY NOTES
16 ABSTRACT
          An  analytical scheme  is presented which permits assessment  of the
   photochemical  significance of light-duty  mobile source  hydrocarbon emissions.
   The scheme incorporates both the  mass  and atmospheric  reactivity of the
   hydrocarbon emissions.  Analytical  procedures supplementary  to  those de-
   fined for light-duty mobile source certification in  the Federal Register are
   defined.  The analytical procedures  permit  definition of four  basic reactivity
   classes of hydrocarbons: Class I,  nonreactive,  including  methane,  ethane,
   acetylene,  propane,  and benzene;  Class II,  reactive, including the C^ and
   higher paraffins;  Class III,  reactive, including the aromatics except  benzene;
   and Class IV,  reactive,  including the olefins.  Procedures for assignment of
   a Hydrocarbon Photochemical  Reactivity  Index utilizing  the reactivity defini-
   tion in conjunction with the mass  of emissions  are described in detail.
17
                             KEY WORDS AND DOCUMENT ANALYSIS
                DESCRIPTORS
                                          b IDENTIFIERS/OPEN ENDED TERMS
                         C  COSATI I'lcld/Croup
   Mobile Sources
   Hydrocarbons
   Photochemical  Reactivity
   Indexing  Procedures
13 DISTRIBUTION STATEMENT
   Release unlimited
19 SECURITY CLASS (This Report)
     none
                         21 NO OF PAGES
28
                                          20 SECURITY CLASS (Thispage)
                                               none
                                                                   22 PRICE
EPA Form 2220-1 (9-73)
                                         23

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