United States      Environmental Sciences Research
         Environmental Protection  Laboratory
         Agency        Research Triangle Park NC 27711
         Research and Development
v>EPA   Environmental
         Sciences Research
         Laboratory Report
         Abstracts

         (October  1978 -
         March 1979)

-------
551557
**"
               UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
                      ENVIRONMENTAL SCIENCES RESEARCH LABORATORY
                              RESEARCH TRIANGLE PARK
                               NORTH CAROLINA 27711
      The Environmental  Sciences Research Laboratory  (ESRL) conducts an
extensive research program on the effects of air  pollution on the atmos-
phere and the subsequent impact on air and water  quality and land use.
Both laboratory and field investigations involving the sciences of
chemistry, physics, and meteorology are used to obtain necessary infor-
mation to quantitate the relationships between emissions of pollutants
from all types of sources and air quality and atmospheric effects.   The
ESRL provides needed techniques and instrumentation for the measurement
a.nd characterization of pollutants in the ambient air and in the emissions
from all types of sources.

      The ESRL Report Abstracts is published semiannually for those  who
are interested in the activities of the Laboratory.  Journal articles or
symposia proceedings are usually available from local  libraries.  EPA
Office of Research and Development reports are available (prepaid) from
the:

               National Technical  Information Service (NTIS)
               U.S.  Department of Commerce
               5285 Port Royal Road
               Springfield, VA  22151
               (Telephone:  703/557-4650)

      Cite the PB number, item 2 on the EPA  Form 2220-1,  when ordering
reports  from  the  NTIS.

      If you  wish to continue receiving these semiannual  reports, or
nominate additional  recipients,  please  fill  in the required  information
below, as well  as  the return  address  block on the reyerse, and return
this sheet to us.
                             QfOtOLM
                              A.  P. Altshuller
                                  Director
                  Environmental  Sciences Research Laboratory
(  )      Please discontinue sending these abstracts to me.

(  )      Please send your semiannual Reports Abstracts to the addressees
        listed below:

-------
 (Please include  ZIP  Code)
                                     U.  S. Environmental Protection Agency
                                     Office of Research and Development
                                     Environmental  Sciences  Research Laboratory
                                     Research Triangle Park, N.C.  27711
Attn: Technical  Information Coordinator
      Mail Drop  59
                       (Fold on dotted line and seal before mailing)

-------
                                   ftCHNICAL REPO 'T DATA
                            , i'h asf read Insl/in lions on tin- ;ci • lfliiifl
 1 REPORT NO
  EPA-600/2-78-007
PB-277.-394
4 TITLE ANOSUBTITLE
  EVALUATION OF A SULFUR  DIOXIDE MASS EMISSION  RATE
  MONITORING SYSTEM
                                                           3 RECIPIENT'S ACCESSION NO
                                                           5 REPORT DATE
                                                            January 1978
                           6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
  Roosevelt Rollins
                                                           8. PERFORMING ORGANIZATION REPORT NO.
9 PERFORMING ORGANIZATION NAMF AND ADDRESS
  Environmental Sciences  Research Laboratory -  RTP,  NC
  Office of Research  and  Development
  U.S. Environmental  Protection Agency
  Research Triangle Park,  NC  27711	
                            1O PROGRAM ELEMENT NO

                              1AD712 BA-18 (FY-77)
                            11 CONTRACT/GRANT NO
 12. SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences  Research Laboratory  -  RTP,  NC
  Office of Research  and  Development
  U.S. Environmental  Protection Agency
  Research Triangle Park,  NC  27711	
                            13 TYPE OF REPORT AND PERIOD COVERED
                               Final 8/76 - 7/77	
                            14. SPONSORING AGENCY CODE
                               EPA/600/09
 15. SUPPLEMENTARY NOTES
 16. ABSTRACT

       An evaluatiqn  was  conducted to determine  the  capabilities and limitations of
  a commercially  available monitoring system  that  provides sulfur dioxide  mass  emission
  rate data as a  direct output.   The monitoring  system was operated continuously for
  extended periods  at a coal-fired power plant and a sulfuric acid production  facility.
  Additional  testing  was  performed at a Simulated  Stationary Source Facility  to confirm
  some deficiencies noted during field operations.   The system's performance was
  verified by comparing its output data with  results using EPA emissions measurement
  reference methods.

       Results are  presented for three performance tests at both field  sites.   For
  the power plant tests,  the monitor agreed within 20% of the accepted  reference
  method.  In the case of the acid plant,  the system accuracy was as poor  at  58%.
  Generally,  the  monitoring system performed  reliably throughout the extended  test
  program.  The system remained operational greater  than 90% of the time during the
  four-month  test period.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
              b.lDENTIFIERS/OPEN ENDED TERMS  C.  COSATI T icId/Croup
  *Air pollution
  *Sulfur dioxide
  *Mass
  *Emission
  *Monitors
  *Evaluation
                                               13B
                                               07B
13 DISTRIBUTION STATEMENT
  RELEASE TO  PUBLIC
                                              19 SECURITY CLASS (This Report I

                                                  IINr.l
                                                                         21 NO. OF PAGES
               20 SECURITY CLASS (Tinspage)
                   UNCLASSIFIED
                                                                         22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPOM
                            (Please read latfnictions on the re\ • • tc
                  DATA
                  before completing)
 REPORT NO
  EPA-600/2-78-060
                                                           3. RECIPIENT'S ACCESSION-NO
PB-280-048
 TITLE AND SUBTITLE
  DEVELOPMENT OF A PORTABLE  DEVICE TO COLLECT
  SULFURIC ACID AEROSOL
  Second Interim Report
                          5. REPORT DATE

                           March 1978
                          6. PERFORMING ORGANIZATION CODE
 AUTHOR(S)
 Herbert C. Miller,  David  W.  Mason and William J. Barrett
                          8. PERFORMING ORGANIZATION REPORT N(
                            3778-XII
                            SORI-EAS-77-731
 PERFORMING ORG tNIZATION NAME AND ADDRESS

  Southern Research  Institute
  2000 Ninth Avenue  South
  Birmingham, Alabama   35205
                          10. PROGRAM ELEMENT NO.

                            1AAS01  CA-20 (FY-78)
                          11. CONTRACT/GRANT NO.
                            68-02-2468
12. SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences  Research Laboratory - RTP.NC
  Office of Research and  Development
  U.S.  Environmental Protection Agency
  Research Triangle Park, NC  27711
                                                            13. TYPE OF REPOR T AND PERIOD COVERED
                            Interim 9/76-9/77
                          14. SPONSORING AGENCY CODE
                            EPA/600/09
15. SUPPLEMENTARY NOTES
  Previous Report:  EPA-600/2-77-027,  February 1977
16. ABSTRACT

       Progress is reported  on research to develop a quantitative,  interference-free
  method for collecting  airborne sulfuric acid aerosol on a  filter.   Since previous
  research found that  severe losses of sulfuric acid were caused  by  ammonia,  ambient
  particulate material,  and  other interferents, a method was  needed  that converts
  sulfuric acid to a stable  derivative for subsequent analysis.   Methods evaluated for
  direct fixation of sulfuric acid aerosol were not found to  be  selective.  Therefore,
  a  sampling method was  investigated that uses a combination  of  selective volatilization
  of the sulfuric acid,  prefiltration of particulate interferents,  and  derivation of the
  vaporized acid on an alkali-impregnated filter.  The initial stages of this current
  research on the volatilization-derivatization technique are described.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                               b.lDENTIFIERS/OPEN ENDED TERMS
                                                                            COSATI Field/Group
  *  Air Pollution
  *  Sulfuric Acid
  *  Aerosol
  *  Collecting Methods
  *  Filters
  *  Tests
                                             13B
                                             07 B
                                             07D
                                             14B
13 DISTRIBUTION STATEMENT


  RELEASE TO PUBLIC


EPA Form 2220-1 (9-73)
             19 SECURITY CLASS (This Report)
               UNCLASSIFIED
                                                                          21 NO OF PAGES
63
             20 SECURITY CLASS (Thispage)
               UNCLASSIFIED
                                        22 PRICE

-------
                                  TECHNICAL Kf OUT HAT A
                           (Please read liutniftio'u mi I'll- f-  ' ••<: before cumpli mix)
1. REPORT NO
  EPA-600/2-78-178
PB-286-939
4 TITLE AND SUBTITLE
 AUTOMATIC INTERFACING SYSTEM  FOR  SAMPLING TOTAL
 MERCURY IN STATIONARY SOURCE  EMISSIONS
7 AUTHOR(S)
 D.  J.  Sibbett and T. R. Quinn
9 PERFORMING ORGANIZATION NAME AND ADDRESS
 Geomet, Incorporated
 2814-A Metropolitan Place
 Pomona, California 91767
12 SPONSORING AGENCY NAME AND ADDRESS
 Environmental Sciences Research  Laboratory - RTP, NC
 Office of Research and Development
 U.S.  Environmental Protection Agency
 Research Triangle Park, N.C. 27711
                                                           3 RECIPIENT'S ACCESSION NO.
                           REPORT DAT F
                          August  1978
                         6 PERFORMING ORGANIZATION CODfc
                                                           8 PERFORMING ORGANIZATION REPORT NO
                                                           10 PROGRAM ELEMENT NO
                            1AD712
BA-11(FY-76)
                         11 CONTRACT/GRANT NO
                                                             68-02-1789
                         13 TYPE OF REPORT AND PERIOD COVERED
                            Final 6/75 - 10/76	
                          14 SPONSORING AGENCY CODE
                            EPA/600/09
15 SUPPLEMENTARY NOTES
16 ABSTRACT
      An interfacing system to sample total  mercury emissions  in  source streams and
 suitably condition, dilute, and  transport the sample to a mercury  measuring instrument
 was designed, fabricated, and tested.   The  system consists of three  components:  a
 conditioner, a diluter, and a pump module.   The conditioner contains a furnace to
 thermally decompose compounds at temperatures up to 1000°C and a liquid scrubbing
 system to remove particulates and interfering gases, such as  sulfur  dioxide and
 nitrogen dioxide.  The diluter module  is  used at sources where mercury levels are
 above the calibration range of the measuring instrument.  The pump module draws the
 sample through the system, exhausts  the waste scrubber liquid, and maintains a con-
 stant pressure in the analyzer-.

      Field tests were conducted  at a coal-fired power plant.   Good correlation was
 obtained between the interface/photomatic analyzer and a reference manual  procedure.
 Instrumental results ranged from 1.74  to  6.96 ug/m3, with mean value of 4.23 pg/m3;
 reference method results varied  from 1.60 to 7.25 yg/m3, with a mean value of 4.66
 gg/m3
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
 *  Air pollution
 *  Mercury (.metal)
 *  Metal  vapors
 *  Hazardous materials
 *  Sampling
 *  Chemical analysis
18 DISTRIBUTION STATEMENT
      RELEASE TO PUBLIC
                                              1) IDENTIFIERS/OPEN ENDED TERMS
                                              '!> SECURITY CLASS (This Report)
                                               UNCLASSIFIED
             (1 SECURITY CLASS (This page)

             IIMPI
                                       c.  COSATI I Icld/Group
                                            13B
                                            07B
                                            11F
                                            11G
                                            14B
                                            07D
                                       21 NO OF PAGES
                                          95
                                                                         22 PRICE
EPA Form 2220-1 (Rev. 4-77)   PREVIOUS EDITION is "i>co.-F r •

-------
                                   TECHNICAL REP"' IT DATA
                            (I'lcaic read Inunctions on //•< r  r*r before comfit tuifl
                                                           3 RECIPIENT'S ACCESSION NO
                                    PB-286-941
 . TITLE AND SUBTITLE
CHEMICAL ANALYSIS OF STATIONARY SOURCE  PARTICULATE
POLLUTANTS  BY MICRO-RAMAN SPECTROSCOPY
 Interim Report      	•
            5 REPORT DATE
              August  1978
            6 PERFORMING ORGANIZATION CODE
 AUTHOR(S)

     E.  S.  Etz,  G.  J.  Rosasco, and  K. F.  J.  Heinrich
                                                           8 PERFORMING ORGANIZATION REPORT NO
 PERFORMING ORGANIZATION NAME AND ADDRESS
Gas and  Particle Science Division
National  Bureau of Standards
Washington,  D.  C.  20234
             10 PROGRAM ELEMENT NO.

               1AD712	BD-Q7   (FY-77)
             11 CONTRACT/GRANT NO
                                                             EPA-IAG-D6-F012
 2 SPONSORING AGENCY»NAME AND ADDRESS
 [nvironmental  Sciences Rese'arch Laboratory -  RTP,  NC
 Jffice of  Research and Development
 J.S. Environmental Protection Agency
Research Triangle Park. N. C. 27711	
             13 TYPE OF REPORT AND PERIOD COVERED

                Interim  4/7fi-3/77	
             14. SPONSORING AGENCY CODE
              EPA/600/09
 5. SUPPLEMENTARY NOTES
 6 ABSTRACT
Analytical  capability to identify the principal  molecular species present in microparti-
cles is demonstrated on the basis of Raman  spectra  of selected compounds and materials.
Among the  inorganic species studied are  sulfates, nitrates,  carbonates and oxides, for
which Raman spectra are discussed for single,  solid particles  of size down to 1  micro-
meter.  The method of micro-Raman analysis  is  applied to  the molecular characterization
of individual  microparticles from power  plant  emissions.   Raman spectra have been ob-
tained from microparticles of oil-fired  power  plant emissions  collected by the EPA with
cascade impaction samplers.

Vanadium pentoxide, V205, has been identified  as a  major  component of microparticles
present in  such  samples.  Th'e presence of certain other vanadium containing species such
as vanadyl,  V02+, and ortho-vanadate, V043~, is  not indicated  from the results of these
neasurements.  Other Raman spectra show  evidence of crystalline sulfate, S042~,  as a
species present  in major proportions.  However,  the exact nature of the associated cat-
ion specie(s)  has not been determined.   Many of  the spectra  obtained from fly ash par-
;icles show Raman bands characteristic of polycrystalline graphite apparently due to
the presence of  carbonaceous material associated with the particles.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lDENTIFIERS/OPEN ENDED TERMS
                            COSATI 1 JCld/Croup
  * Air  pollution
  * Particles
  * Chemical  analysis
  * Raman spectroscopy
  * Vanadium oxides
  * Sulfates
                              13B
                              07D
                              14B
                              07B
 18. DISTRIBUTION STATEMENT


     RELEASE TO PUBLIC
19 SECURITY CLASS (This Report)

   UNCLASSIFIED	
                                                                         21 NO OF PAGES
46
20 SECURITY CLASS (This page)
   UNCLASSIFIED
                          22 PRICE
 EPA Form 2220-1 (Rev. 4-77)   PREVIOUS EDITION is OBSOLETE

-------
                                  TECHNICAL REPORT DATA
                           (Please read Instructions on the ic\ cm before eomplftuigj
1 REPORT NO
  EPA-600/2-78-194
                                   PB-288-512
                                                           3 RECIPIENT'S ACCESSION NO
4. TITLE AND SUBTITLE
 X-RAY ANALYSIS OF AIRBORNE ASBESTOS
 Final Report:   Design and Construction of a
 Prototype Asbestos Analyzer	
             5 REPORT DATE
               August 1978
             6 PERFORMING ORGANIZATION CODE
7. AUTHOR(S)
                                                           8 PERFORMING ORGANIZATION REPORT NO
 L.  S.  Birks,  J.  V.  Gilfrich, and J. W. Sandelin
9 PERFORMING ORGANIZATION NAME AND ADDRESS

 Radiation Technology Division
 Naval  Research Laboratory
 Washington,  D.  C.   20375
             10 PROGRAM ELEMENT NO

              1AD712 BA-25  (FY-77)
             11  CONTRACT/GRANT NO.
                                                            EPA-IAG-D6-0651
12. SPONSORING AGENCY NAME AND ADDRESS
 Environmental  Sciences Research Laboratory  -  RTP,  NC
 Office of Research and Development
 U.  S.  Environmental Protection Agency
 Research Triangle Park, N.C.  27711
             13 TYPE OF REPORT AND PERIOD COVERED

              Final   10/76-6/78	
             14 SPONSORING AGENCY CODE
              EPA/600/09
15. SUPPLEMENTARY NOTES
16 ABSTRACT
      A prototype asbestos analyzer has been  designed and constructed for use by  the
 Environmental  Protection Agency.  It incorporates  the principle of broad-beam  x-ray
 optics and the special fiber-aligned sample  described in earlier reports (EPA-650/2-
 75-004 and EPA-600/2-77-062).  The prototype instrument utilizes two detectors for
 simultaneous measurement of diffracted signal  and  background; the mass of asbestos is
 simply the net difference in intensity for these  two detectors normalized by the
 sensitivity of the analyzer as determined using  standards.

      The prototype analyzer is contained in  a  vacuum box 15x15x32 cm and mounts  on
 top of a standard commercial x-ray power supply.   It uses a Cr target spectrographic
 tube which is  located in a separate lead-shielded  enclosure in the box.  The mechanics
 of selecting the 20 diffracting angles for different forms  of asbestos are unique and
 especially designed to minimize the space required.   The beam trap is a critical
 component of the instrument; it reduces the  backscattered noise signal to less than
 100 photons/sec from an incident beam of about 10''  photons/sec.

      Preliminary tests with the analyzer indicate  a  sensitivity of 18 photons  per
 second per yg  of chrysotile and a calculated 3a  detection limit of 0.1 pg for  a  500
 second measurements.  Amosite has a somewhat better  sensitivity and detection  limit.
17.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
b IDENTIFIERS/OPEN ENDED TERMS  C  COSATI 1 ICld/Group
 * Air  pollution
 * Asbestos
 * Analyzers
  Design
 * X-ray diffraction
  Alignment
  Quantitative  analysis
 Chrysotile
 Amosite
13B
08G
HE
14B
20F
07D
18 DISTRIBUTION STATEMENT
 RELEASE TO PUBLIC
                                              19 SECURITY CLASS (Tins Report)
                                               UNCLASSIFIED
                           21 NO OF PAGES

                              25	
                                              20 SECURITY CLASS (Tinspage)

                                               UNCLASSIFIED
                                                                        22 PRICE
EPA Foim 2220-1 (Rev. 4-77)
                      PREVIOUS EDITION IS OBSOLETE

-------
                                   TECHNICAL HEPORT DATA
                            (1 It o\r rcatl Instructions on tin rc.ii«• before tumpl- IIIIK)
EPA
      -600/2-78-197 ______    PB:291-132
4 TITLfc AND SUBTITLh
   CALIBRATION STANDARDS FOR  X-RAY  SPECTROMETERS USED
   FOR  POLLUTION SAMPLE ANALYSIS
                                                           3 RECIPIENT'S ACCESSION NO.
                                                         5 REPORT DATE
                                                           September 1978
                                                         6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
                                                            I. PERFORMING ORGANIZATION REPORT NO
                           R.A.  Semmler  and R.G. Draftz
3 PERFORMING ORGANIZATION NAME AND ADDRESS
                                                           10 PROGRAM ELEMENT NO
    I IT  Research Institute
    10 West 35th Street
    Chicago, Illinois 60616
                                                               1AD712  BD-07(FY-76)
                                                         11 CONTRACT/GRANT NO
                                                               68-02-1734
12 SPONSORING AGENCY NAME AND ADDRESS
   Environmental  Sciences Research Laboratory - RTP, NC
   Office  of Research and Development
   U.S.  Environmental Protection  Agency
   Research Triangle Park, N.C. 27711	
                                                         13 TYPE OF REPORT AND PERIOD COVERCD
                                                         	Final       8/75 - 3/77
                                                         14 SPONSORING AGENCY CODE

                                                            EPA/600/09
15 SUPPLEMENTARY NOTES
16 ABSTRACT

         A  technique is described  for making aerosol standards for x-ray fluorescence
   analysis  by depositing sized particles suspended in a carrier solution onto  the
   surface of a polycarbonate  filter.   Size is controlled by a separate sedimentation
   step  following grinding  in  a boron carbide mortar and pestle.  Binding of  the
   deposition to the filter  is accomplished by a collodion film layer applied both
   before  and after the particle  deposition.  The deposited mass is determined
   gravimetrically from a companion filter prepared from a large volume aliquot of
   carrier solution and without collodion.  Standards for 18 different elements have
   been  prepared.
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
 Air  pollution
 Aerosols
*Calibrating
*Standards
 Xray spectrometers
 Xray fluorescence
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                                                      C  COSATI I IcIJ/Group
                                                                         13B
                                                                         07D
                                                                         14B
                                                                         20F
18 DISTRIBUTION STATEMENT


   RELEASE  TO  PUBLIC
                                            19 SECURITY CLASS (FhHReport)
                                                UNCLASSIFIED
21 NO. OF PAGES

   51	
                                            20 SECURITY CLASS (Tins page I

                                                UNCLASSIFIED
                                                                      22 PRICE
EPA Fo.m 2220-1 (Rev 4-77)
                              t 01 T ION li OBSOLETE

-------
TECHNICAL REPORT DATA
(Please read Instructions on the i, wrse before completing)
1 REPORT NO
EPA-600/2-78-212
4 TITLE AND SUBTITLE
INVESTIGATION OF PARTI CULATE
CONTACT ELECTRICITY
Final "Report
7 AUTHOR(S)
Walter John, Georg Reischl,
Jerome J. Weslowski
2
PB-289-565
MATTER MONITOR I
3. RECIPIENT'S ACCESSION NO
5 REPORT DATE
NT, IKING October 1978

6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO
William Devor, and
9 PERFORMING ORGANIZATION NAME AND ADDRESS
Air and Industrial Hygiene Laboratory
California Department of Health
2151 Berkeley Way
Berkeley, California 94704
12 SPONSORING AGENCY NAME AND ADDRESS
Environmental Sciences Research Laboratory -
Office of Research and Development
U.S. Environmental Protection Agency
Research Triangle Park, N. C. 27711
15. SUPPLEMENTARY NOTES
Previous Repo'rt: EPA-650/2-75-043, February
10. PROGRAM ELEMENT NO.
1AD712 BA-04 (FY-77)
11. CONTRACT/GRANT NO.
R 803719-01-2
13. TYPE OF REPORT AND PERIOD COVERED
RTP, NT. Final
14. SPONSORING AGENCY CODE
EPA/600/09
1975

16 ABSTRACT
To better understand the contact electrification monitor for particulate matter, charge
transfer by aerosol particles impacting on metal surfaces has been investigated. Mono-
disperse, uniformly charged or neutral aerosol particles (1-5 pm diameter) from a
vibrating orifice or fluidized bed generator were bounced on a metal probe. The trans-
fer of precharge from the particles was found to be a sensitive indicator of the probe
surface condition. A surface preparation procedure was developed which yielded linear
charge transfer curves.
Measurements were made of methylene blue, potassium biphthalate, sodium chloride and
aluminum particles impacting on stainless steel, Inconel, titanium, and platinum
probes. For insulating materials, the transfer of precharge was independent of par-
ticle size while the contact charge was proportional to the cube of particle diameter
and directly proportional to impact velocity. The magnitude of the contact charge was
strongly dependent on the electrical resistivity of the material. A theoretical model
was found to account semi -quantitatively for all aspects of the data. A major remain-
ing difficulty is the lack of knowledge of the contact potential. The implications of
these findings for monitoring applications are discussed in detail and the advantages
and disadvantages of the monitor are assessed.
17.
KEY WORDS AND DOCUMENT ANALYSIS
a DESCRIPTORS
*Air pollution
*Aerosols
*Particles
*Monitors
*Contact potentials
*Evaluation
IS. DISTRIBUTION STATEMENT
, RELEASE TO PUBLIC
b.lOENTIFIERS/OPEN ENDED TERMS

19 SECURITY CLASS (This Report/
UNCLASSIFIED
20 SECURITY CLASS (Tins page/
UNCLASSIFIED
c. COSATI 1-icld/Group
13B
07D
21 NO OF PAGES
80
22 PRICE
EPA Form 2220-1 (Rev. 4-77)    PREVIOUS EDITION is OBSOLETE

-------
                                   TECHNICAL REPORT DATA
                           (Please read luslnictions on the ri i cisc
 REPORT NO
 EPA-60Q/3-78-100
                                  PB-289-925
4. TITLE AND SUBTITLE

 GLOBAL  DISTRIBUTION OF SELECTED HALOCARBONS,  HYDRO-
 CARBONS,  SFA, AND NO
                                                          3 RECIPIENT'S ACCESSION-NO
                                                          5 REPORT DATE
                                                            Dprpmhpr 1978
                                                          6 PERFORMING ORGANIZATION CODE
 Hanwant  B.  Singh,  L.J. Salas, H.  Shigeishi,  and
 E. Scribner
                                                          8. PERFORMING ORGANIZATION REPORT NO
 PERFORMING ORGANIZATION NAME AND ADDRESS
 SRI International
 Menlo Park,  California  94025
                                                           10. PROGRAM ELEMENT NO.
                                                              1AA603 AI-02   (FY-77)
                                                          11 CONTRACT/GRANT NO
                                                             8038020-02
12 SPONSORING AGENCY NAME AND ADDRESS
 Environmental Sciences Research  Laboratory-RTF,NC
 Office  of  Research and Development
 U.S.  Environmental Protection  Agency
 Research Triangle Park, North  Carolina  27711	
                                                           13 TYPE OF REPORT AND PERIOD COVERED
                                                            Interim 7/77 -  3/78
                                                           14 SPONSORING AGENCY CODE
                                                             EPA/600/09
15. SUPPLEMENTARY NOTES
16. ABSTRACT
       Northern and Southern  hemispheric distributions of halogenated species, hydro-
  carbons, SF, and N?0 ase presented.   The atmospheric growth rates of selected halo-
  carbons and N?0 are characterized.   The fluorocarbon 11 and 12 global burden and
  hemispheric distribution is consistent with the view that no significant sinks in
  the  troposphere exist.  The north-south gradients of fluorocarbon 11, 12, 113, 114,
  CC1, ,  and SFfi suggest rapid global  mixing with an interhemispheric exchange rate
  of about one year.  Within  each hemisphere, these species are well mixed.  N20 shows
  the  least variations around the globe.  The global distribution of CH_CC1_ is found
  to be complex and suggests  higher HO levels in the southern hemisphere and around
  the  equator, when compared  to the northern hemispheric HO levels.  The global
  distribution of CH.C1 is almost uniform and a significant natural source has been
  identified in the ocean.  It is also shown that largs  anthropogenic primary or
            sources of CH Cl  and CC1   exist.  Species such as CHC1_, CH2C12' C2HC13'
  and  C.C1. show very larg*e north-soQth gradients.  The atmospheric growth of Eluoro-
  secondary sources  of  CH^Cl and CC1
  and C Cl  show very la
  carbons il, 12, CH CC1
  these constituents;
                         3'
                            and CC1,  appear to be consistent with the emissions of
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                                                        c. COSATI Field/Group
  *  Air pollution
  *  Halohydrocarbons
  *  Chemical analysis
     Troposphere
                                                                          13B
                                                                          07C
                                                                          07D
                                                                          04A
IS DISTRIBUTION STATEMENT

  RELEASE TO PUBLIC
                                              19 SECURITY CLASS (This Report i

                                               ITMrT.ASSTFTF.n	
                                                                        21 NO. OF PAGES
81
                                              20 SECURITY CLASS (Thispage)
                                               UNCLASSIFIED
                                                                        22 PRICE
EPA Form 2220-1 (9-73)

-------
r
                           (I'1! J\
                                DATA
                    l">n\ on ill: Hi ''< hi lui, i •»•;; .', i
 1 REPORT NO
   EPA-600/2-79-004
ziz:
PB-290-658
 4 TITLE AND SUBTITLE
  EVALUATION OF TECHNIQUES OFR MEASURING BIOGCMIC
  AIRBORNE SULFUR COMPOUNDS
  Cedar Island Field Study 1977    	   	
i  rLCII'ir NTS AJC--S..SON NO


5  RCPGR' DAT I-.-


6  PE~RFOHMil\:G OHGAN!2MTIO.M CO fit
                                                      "1
                                                      -i
 7 AUTHOR(S)
  W.A. McClenny, R.W. Shaw, R.E. Baumgardner, R. Paur
  and A. Coleman
                                                          8 I'ERi'ORMING ORGANISATION HLI'OHT NO
 9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Environmental Sciences Research Laboratory
  Office of Research and Development
  U.S. Environmental Protection Agency
  Research Triangle Park, N.C. 27711    	
 12 SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences Research Laboratory  — RTP, NC
  Office of Research and Development
  U.S. Environmental Protection Agency
  Research Triangle Park, N.C. 27711
                                        10 PROGRAM ELEMENT NO
                                         1AD712  BB-12. 16. & 17(FY-78
                                        11 CONTRACT/GRANT NO
                                        13 TYPE OF RCPORT AND PERIOD COVERED
                                            In-house
                                        14 SPONSORING AGENCY CODE
                                           EPA/600/09
 15 SUPPLEMENTARY NOTES
 16 ABSTRACT

       Sulfur in both gaseous and particulate form has been measured near biogenic
  sources using new measurement techniques. The preconcentration of gaseous sulfur on
  gold-coated glass beads followed by desorption into a flame photometric detection for
  sulfur is shown to have a detection limit of 0.1-0.2 ng of sulfur and to allow for
  speciation of H2S, CH3SH and (CH )2S at low parts per trillion levels.  Ambient
  levels of NO- and 0  were found to alter the molecular form of^sulfur on the beads
  unless scruboed from the sampled air.  A collection technique using tandem filters is
  extended from earlier efforts on fine and coarse aerosol to include collection of S09
  and H2S on chemically coated filters; these filters are analyzed by X-ray
  fluorescence for sulfur content. Measurements of gases evolved from biogenic sources
  reveal E^S and (CH^^S as primary components with significant diurnal variations.
  Recommendations for further instrument development are given.
 17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
  *Air pollution           *F.v.iluntion
  *Sulfur inorganic compounds
  •:Sulfur organic compounds
  ^Biological productivity
  ACoasts
  Measurement
  *Chemical  Analysis
                                              b IDENTIFIERS/OPEN LNDtD TERMS
                            Cednr Island, NC
                                         COSATI I iclil;(>ruu|>

                                            13R
                                            07 H
                                            07C
                                            08A
                                            08 F
                                            07D
 18 DISTRIBUTION STATLMCNT
  RELEASE TO PUBLIC
                           19 SECURITY CLASS 11 ln\ Krporl)
                                 UNCLASSIFIED
                                       21  NO OF PAGfcS
                                          138
                           2O SECURITY CLASS i / Ins pm'i.
                                 UNCLASSIFIED
                                                                        22 PRICE
 EPA Form 2210-1 (Rev 4-77)
                                    IS Oi'SOLt- ft.

-------
                                   TECHNICAL REPORT DATA
                            (I'lcasc read Instructions on lite reverse before completing/
  BEPOHT NO
 EPA-600/2-79-005
                                PB-290-909
4. TITLE AND SUBTITLE
  EXAMINATION OF AUTOMATIC DATA REDUCTION METHODS FOR
  PARTICLE FIELD HOLOGRAMS
                                                           3 RECIPIENT'S ACCESSION NO.
                                                           5 REPORT DATE
                                                            January  1979
                                                           S-JPERFORMING ORGANIZATION CODE
  AUTHOR(S)
  J.D.  Trolinger
                                                           8. PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Soectron Development Laboratories, Inc.
  3303 Harbor Boulevard
  Costa Mesa, CA 92626
                                                           10 PROGRAM ELEMENT NO.
1AD717 BF-A8
                                                                                771
                                                           11. CONTRACT/GRANT NO.
                                                                 68-02-2491
12 SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences Research Laboratory — RTF, NC
  Office of Research and Development
  U.S.  Environmental Protection  Agency
  Research Triangle Park.  N.C. 27711	
                                                           13 TYPE OF REPORT AND PERIOD COVERED
                                                             Final       0/"  n "°
                                                           14. SPONSORING AGENCY CODE
                                                               EPA/600/09
15. SUPPLEMENTARY NOTES
16. ABSTRACT
        Holographic recording  techniques provide one of the most powerful particle
   field diagnostic tools  in existence.   A hologram can provide a frozen
   three-dimensional image of  a  particle field through which detailed microscopic
   examination of individual particles is possibe. Frequently, a particle field may
   contain many thousands  of particles,  and it becomes impractical for the human
   operator to glean all the data of interest from such a hologram.  For holography to
   reach its full potential in particle  diagnostics, a three-dimensional image analyzer
   is required.
        The purpose of this study was to examine the feasibility of using existing
   electro-optic image analyzers to automatically analyze three-dimensional image
   fields and to determine what  modifications of existing equipment would be required
   to construct such a system.
        Sample holograms as well as holograms produced in an actual field holo-camera
   were used to make the evaluations experimentally, and well-refined analytical
   descriptions of holographic images were used to add to the understanding of system
   requirements. The study established that existing image Analyzers are capable within
   useful practical limits of  locating particle images in three-dimensions and
   measuring size and shape factors of the particle.  A plan for integrating such
   equipment to produce a  fully  automated data reduction system is presented.	
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                                                         c. COSATI I icIcl/Group
 *Air pollution
 *Particles
  Examination
 *Data reduction
 *Analyzers
 *Holography
                                                                             13B
                                                                             14B
                                                                             09B
                                                                             14E
 18 DISTRIBUTION STATEMENT


  RELEASE TO PUBLIC
                                               19 SECURITY CLASS (1 his Keport)
                                                UNCLASSIFIED	
          21 NO OF PAGES
          	59
                                                                         22 PRICE
 EPA Form 2220-1 (Rev. 4-77)   PREVIOUS COITION is OBSOLETE

-------
                                   TECHNICAL REPORT DATA
                           (I'lease read Inuruciions on llic reverse fie fun t01
1. HEPUHT NO
 EPA-600/2-79-017
PB-292-093
4 TITLE AND SUBTITLE

 ANALYTICAL  PROCEDURES FOR CHARACTERIZING UNREGULATED
 POLLUTANT EMISSIONS FROM MOTOR VEHICLES
                           j RECIPIENT'S ACCESSION NO.
                           5. REPORT DAI E
                            February 1979
                           6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
  Harry Dietzman,  Lawrence Smith, Mary Parness,
  and Robert  Fanick
                          8 PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
 Southwest Research Institute
 8500 Culebra  Road
 San Antonio,  Texas 78284
                                                           1O PROGRAM ELEMENT NO
                               1AA601  CA-11 (FY-78)
                           11 CONTRACT/GRANT NO.

                               68-02-2497
12 SPONSORING AGENCY NAME AND ADDRESS
 Environmental  Sciences and Research Laboratory  -  RTP,  N(
 Office of  Research and Development
 Environmental  Protection Agency
 Research Triangle Park, N.C. 27711
                           13 TYPE OF REPORT AND PERIOD COVERED
                               Interim 3/77 - 10/78	
                           14 SPONSORING AGENCY CODE
                               EPA/ 600/09
IS SUPPLEMEN FAHY NOTES
16 ABSTRACT
    Analytical  procedures are described that may  be  used to assess motor
    vehicle emission  rates of several unregulated pollutants including
    aldehydes,  organic amines, sulfur dioxide, nitrous  oxide, several individual
    hydrocarbons  including benzene, hydrogen sulfide, total  cyanide, organic
    sulfides, nickel  carbonyl, ammonia, sulfate,  and N-nitrosodimethylamine
    (sampling conditions only).   A series of validation experiments involving
    motor vehicle exhaust with injects of known quantities of the compounds
    of interest and the Constant Volume Sampling  system commonly used in
    emissions certification are described for several of the analytical
    procedures.   The  Clean Air Act as amended August 1977 requires in section
    202(a) 4 that unregulated pollutants emitted  from motor vehicles be
    measured to assure that no unreasonable risk  to  public health and
    welfare exists.
17
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
   Air  pollution
   Motor  vehicles
   Exhaust  emissions
   Chemical  analysis
   Reviews
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                        C  COSATI 1 Icld/Group
                                            13B
                                            13F
                                            21B
                                            07D
                                            05B
18 DISTRIBUTION STATEMENT

    RELEASE  TO PUBLIC
              19 SECURITY CLASS (Ilia Report)
                UNCLASSIFIED
21 NO Of PAGES

  495	
                                              20 SECURITY CLASS (This page/

                                                 UNCLASSIFIED
                                                                         22 PRICE
EPA Form 2220-1
              ,. 4-77)
                      PREVIOUS EOlTiOM ,S O13SOL1 Tt

-------
                                   TECHNICAL REPORT DATA
                            (Please read Insane nuns on l/ii! t'.irrsc bctori coinpli tingl
REPORT NO
EPA-600/2-79-
               P_22	f_PB-
                                                           3 RECIPIENT'S ACCESSION NO
4 TITLE AND SUBTITLE
MULTIWAVELENGTH TRANSMISSOMETER  FOR MEASURING MASS
CONCENTRATION OF PARTICULATE  EMISSIONS
                                                         5 RtPOHT DATC
                                                          February 1979
                                                         6. PERFORMING ORGANIZATION CODE
  AUTHOR(S)

Eli  Reisman
                                                           8 PERFORMING ORGANIZATION REPORT NO
0 PERFORMING ORGANIZATION NAME AND ADDRESS
 Ford Aerospace and Communications  Corporation
 Aeronutronic Division
 Newport  Beach, California 92663
                                                          10 PROGRAM ELEMENT NO

                                                           1AA010  (1AD712)
                                                          11 CONTRACT/GRANT NO.
                                                             68-02-2206
12 SPONSORING AGENCY NAME AND ADDRESS
Environmental  Sciences Research  Laboratory - RTP, NC
Dffice  of Research and Development
U.S.  Environmental Protection  Agency
Research  Triangle Park, N.C. 27711
                                                          13. TYPE OF REPORT AND PERIOD COVERED

                                                           Fi na]	7/75 -  5/78	
                                                          14 SPONSORING AGENCY CODE
                                                           EPA/600/09
15 SUPPLEMENTARY NOTES
16 ABSTRACT
A multiwavelength transmissometer  potentially capable of making near-real-time
measurements of particulate mass concentration in industrial stacks was developed.
A computer program is employed  to  interpret the transmissometer data and translate
the  results into mass concentration.   The transmissometer utilizes four different
wavelengths and records the opacity of the particulate emissions at each wavelength.
Since  the response at each wavelength depends on the size of the particles, the rela-
tive values of opacity provide  the computer with information on particle sizes.  If
the  computer is also given the  wavelength dependence of the optical indices of refrac-
tion and  guidelines as to the most probable distribution forms, the computer can
adjust the mean and spread of the  distribution to find a best fit to the experimental
data.   It then uses this information  to compute the mass concentration.  The theory
behind the measurement technique,  a laboratory demonstration of the technique, and
the  optical and electrical design  of  the instrument are discussed.
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
    Air  pollution
    Flue dust
    Particles
    Weight (mass)
    Transmissometers
    Computers
                                              b IDENTIFIERS/OPEN ENDED TERMS  C  COSATI I Icld/Croup
                                                                            13B
                                                                            21B
                                                                            14B
                                                                            09B
 18 DISTRIBUTION STATEMENT
     RELEASE TO PUBLIC
                                               19 SECURITY CLASS (Tins Report)

                                                  UNCLASSTFTFD	
                                                                       21 NO OF PAGES

                                                                         63
                                             20 SECURITY CLASS (Tinspage)
                                                UNCLASSIFIED
                                                                         22 PRICE
 EPA Form 2220-1 (Rev. 4-77)
                       PREVIOUS EDITION IS OBSOL-CTE

-------
  RCPORT NO               ~~~  IT"
   EPA-600/2-79-023	_J
                                   TECHNICAL REPORT DATA
                            (Pica* ri-aii Instruction* on tin- r crtc he/ore completing!
PB-292-331
«S TITLE AND SUBTITLE
CONTINUOUS  READING LIDAR TECHNIQUE FOR MEASURING  PLUME
OPACITY
7 AUTHOR(S)
Dilip G. Saraf
                                                           8. PERFORMING ORGANIZATION REPORT NO
                           RECIPIINT'S ACCESSION NO
                         5 REPORT DATE

                            Feb.ru ajry_19_7?_
                         6 PERFORMING ORGANIZATION CODE
9 PERFORMING ORGANIZATION NAME AND ADDRESS
SRI International
333 Ravenswood  Avenue
Menlo Park, California  94025
                         10 PROGRAM ELEMENT NO

                         _1AD605_  BA-63 (FY-76)
                         11 CONTRACT /GRANT"RJO
                                                             68-02-1291
 12 SPONSORING AGENCY NAME AND ADDRESS
Environmental  Sciences  Research Laboratory-RTP, NC
Dffice of Research  and  Development
J.S. Environmental  Protection Agency
Research Triangle Park,  N.C.  27711
                         13 TYPE OF REPORT AND PERIOD COVERED
                           Final  6/74 - 9/76
                         14 SPONSORING AGENCY CODE
                           EFA/600/09
15 SUPPLEMENTARY NOTES
16 ABSTRACT                                                     	
The development of  a  laser radar (lidar) instrument  for  remote measurement of the opa-
city of smoke-stack plumes is described.  The work was conducted within a number of  con-
straints.  The constraints required the lidar instrument to be field-portable, eye safe,
relatively low in cost,  and simple to operate.  Two  lidar measurement methods were
studied for the instrument:  continuous wave  (CW) lidar  and high pulse rate lidar.

A research model CW lidar was constructed and evaluated.   The evaluation showed that the
CW lidar could remotely  measure the opacities of screen  targets or smoke generator
plumes at night to  within 3% opacity at a distance of approximately 80 meters.  Environ-
mental light interference prevented operation of the lidar during daytime.

3roof-of-principle  experiments were performed to demonstrate the feasibility of using a
ligh pulse rate lidar for plume opacity measurements.  The evaluation showed that the
lidar1s laser did not have enough power to make measurements under field conditions.
However, the lidar  was capable of measuring the opacity  of the screen targets at close
range (40m) and by  placing a small  artificial scattering target in the atmosphere
behind them.  With  this  artificial  signal enhancement, results showed that the high
Dulse rate lidar could remotely measure the opacities of the screen targets to within
2% opacity during daytime or nighttime operation.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b IDENTIFIERS/OPEN ENDED TERMS C.  COSATI Held/Group
 * Air pollution
 * Plumes
 * Opacity
 * Measuring instruments
 * Optical radar
   Development
                                           13B
                                           21B
                                           14B
                                           17H
   Evaluation
 8 DISTRIBUTION STATEMENT
     RELEASE 10 PUBLIC
                                              19 SECURITY CLASS (Tins Report}

                                              IINr.l ASSTFTFD	
                                                                         21 NO. OF PAGES
                                          54
            20 SECURITY CLASS (Thispage)
            UNCLASSIFIED
                                       22 PRICE
EPA Form 2220-1 (Rev. 4-77)   PREVIOUS EDITION is OBSOLETE

-------
                                   TECHNICAL REPORT DATA
                              usi read l'i\lnicluiiH on tilt ri irwr hi fore
  RETORT NO
  EPA-600/2-79-041	
                                                           3 RECIPIENT'S ACCESSION NO
                                PB-292-380
4 TITLE AND SUBTITLE
CHEMICAL COMPOSITION OF EXHAUST  PARTICLES
FROM  GAS TURBINE ENGINES
                                                         5 REPORT DATE
                                                           February 1979
                                                           6 PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
  D.J.  Robertson, J.H. Elwood  and  R.H.  Groth
                                                           8 PERFORMING ORGANIZATION REPORT NO.
9 PERFORMING ORGANIZATION NAME AND ADDRESS
  United Technologies Corporation
  Pratt & Whitney Aircraft Group
  Commercial Products Division
  East  Hartford, Connecticut  06108
                                                         10 PROGRAM ELEMENT NO.

                                                           1AD712  BC-42  (FY-78)
                                                         11 CONTRACT/GRANT NO
                                                          Contract No.   68-02-2458
12. SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences Research  Laboratory—RTP, NC
  Office  of Research and Development
  U.S.  Environmental Protection Agency
  Research Triangle Park, N.C. 27711	
                                                         13. TYPE OF REPORT AND PERIOD COVERED
                                                          Final 11/76 -
                                                         14. SPONSORING AGENCY CODE
                                                         EPA/600/09
15 SUPPLEMENTARY NOTES
16 ABSTRACT
  A program was conducted to chemically  characterize particulate emissions from a
  current  technology, high population, gas  turbine  engine.   Attention was focused
  on polynuclear aromatic compounds, phenols,  nitrosamines  and total organics.   Poly-
  nuclear  aromatic hydrocarbons  (PAH) were  determined by HPLC, GC/MS and NMR techniques.
  Phenols  and  nitrosamines were  isolated and then measured  by gas chromatographic
  methods  utilizing flame ionization detection and  nitrogen detection.   Total
  organics were determined by a  backflush chromatographic procedure.  The particulate
  matter was collected using a high capacity pumping system incorporating 293 mm
  diameter Teflon filters through which  was passed  up to 43 m  of exhaust gas.
  Extraction of the organic matter was performed in a Soxhlet extractor using hexane.
  The engine was operated at idle, approach, climb  and take-off power settings  with
  low sulfur (0.007%S) and high  sulfur (0.25%S) fuels.   Most of the PAH were small
  3-to-4 fused ring species.  No nitrosamines  were  found and except in  a few cases,
  at low levels,  no phenols.  PAH and total organic levels  decreased with increasing
  power setting and were more concentrated  in  the exhaust from the low  sulfur fuel.
  Less than  1% of the organic matter emitted from the engine was adsorbed on the
  particulate  matter.
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                            * Nitroso compounc
                            * Phenols
*  Air pollution
*  Gas turbine  engines
* Exhaust emissions
* Particles
* Chemical composition
* Chemical analysis
* Aromatic polycyclic hydrocarbons
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                                                      i.  COSATl I iclJ/(Jroup
 13B
 2 IE
 21B
 07D
 07C
 18 DISTRIBUTION STATEMENT
   RELEASE TO PUBLIC
                                            19 SECURITY CLASS (This Keport)

                                              UNCLASSIFIED	
21 NO OF PAGES

 178	
                                            20 SECURITY CLASS (I'lii

                                              UNCLASSIFIED
                                                                         22 PRICE
 EPA Form 2220.1 (Re. 4-77)
                       PREVIOUS EDC TION I S OBSOLETE

-------
                                  TECHNICAL REPORT DATA
                           (Please read /HZlntctions on the rci crsc before completing)
 REPORT NO
   EPA-600/2-79-042
                                                          3 RECIPIENT'S ACCESSION-NO.
 TITLE AND SUBTITLE
METHODOLOGY FOR COLLECTING AND ANALYZING ORGANIC
AIR  POLLUTANTS
                                                          5 REPORT DATE
                                                          6. PERFORMING ORGANIZATION CODE
                                                                ruary 1979
 AUTHOR(S)
                                                          8. PERFORMING ORGANIZATION REPORT NO.
Corazon Hastings Vogt
 PERFORMING ORGANIZATION NAME AND ADDRESS

 Environmental Trace Substances  Research Center
 Columbia, Missouri  65201
                                                          10. PROGRAM ELEMENT NO.

                                                              1AA001   (FY-75)
                                                          11 CONTRACT/GRANT NO.

                                                             801050
2 SPONSORING AGENCY NAME AND ADDRESS
 Environmental  Sciences Research Laboratory - RTP, NC
 Office  of Research and Development
 U.  S. Environmental Protection Agency
 Research Triangle Park. NC  27711	
                                                           13. TYPE OF REPORT AND PERIOD COVERED
                                                              Final    	
                                                           14. SPONSORING AGENCY CODE
                                                              EPA/600/09
5. SUPPLEMENTARY NOTES
6. ABSTRACT
      A number of  support-bonded liquid phase  sorption media were developed and
 evaluated in model  systems for collecting and analyzing organic air  pollutants.
 Polymers with various  functional groups were  synthesized and chemically  bonded onto
 inert supports  in thick layers.  A media consisting of a silicone liquid bonded to
 Chromosorb W was  used  with excellent results.  Retention times of most organic
 compounds on this liquid are extremely long at ambient temperatures, and sampling can
 be carried out  for 24  hours at a rate of 10 liters of air per minute.   In contrast,
 subsequent counter current liquid extraction  takes only a few minutes  since retention
 volumes are very  small.  Extracts were analyzed largely by gas chromatography.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b IDENTIFIERS/OPEN ENOEDTERMS
  *  Air pollution
  *  Organic compounds
  *  Collecting methods
  *  Sorption
  *  Chemical analysis
  *  Gas chromatography
                                                                           COSATI I icId/Group
                                                                          13B
                                                                          07C
                                                                          14B
                                                                          07D
18 DISTRIBUTION STATEMENT


  RELEASE TO PUBLIC
                                              19 SECURITY CLASS (This Report)
                                               UNCLASSIFIED
21 NO OF PAGES

 M.
                                              20 SECURITY CLASS (Tins page)
                                               UNCLASSIFIED
                                                                         22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REP' 'IT DATA
                               if rcaJ InHiucnons on ilic i  in before cuiii/'lcti>ig}
1  REPORT NO
      EPA  600/3-78-031
PB-280-050
                                                           3 RECIPIENT'S ACCESSION-NO
4 TITLE AMDSUBTITLE

  ORGANIC  CHARACTERIZATION OF  AEROSOLS AND VAPOR
  PHASE  COMPOUNDS IN URBAN ATMOSPHERES
                          5 REPORT DATE
                              March 1978
                          6 PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
  G.D.  Mendenhall, P.W. Jones,  P.E.  Strup and
  W.L.  Margard	
                                                           8 PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Battel]e Columbus Laboratories
  505  King Avenue
  Columbus, Ohio  43201
                          10 PROGRAM ELEMENT NO
                             1AD712   BD-21  (FY-77)
                           11 CONTRACT/GRANT NO
                             68-02-1409
12 SPONSORING AGENCY N/lMfc AND ADDRESS
   Environmental Sciences  Research Laboratory - RTP, NC
   Office of Research and  Development
   U.S.  Environmental Protection Agency
   Research Triangle Park,  North Carolina  27711	
                           13 TYPE OF REPORT AND PERIOD COVERED
                             Final	
                           14 SPONSORING AGENCY CODE

                             EPA/600/09
15 SUPPLEMENTARY NOTES
16. ABSTRACT

        Organic pollutants  in  urban atmospheres were characterized by analyzing
   particulate and/or vapor-phase samples collected by EPA in St. Louis, Missouri;
   Miami,  Florida; Denver,  Colorado;  Houston, Texas; and at the General Motors Test
   Track in Milford, Michigan.   The particulate samples were extracted with solvents
   and  the extractable materials analyzed by elemental combustion analysis and
   infrared spectroscopic analysis.  To evaluate more than one solvent extraction
   technique, the particulate  samples were aliquoted and analyzed by several  extraction
   procedures.  Some of  the problems encountered with these procedures are discussed.
   Vapor-phase samples were collected on Chromosorb 102 chromatographic traps and
   analyzed using qualitative  gas chromatography-mass spectrometry analysis.  Individual
   species tentatively identified are shown on reconstructed gas chromatograms and
   individual mass spectra  for all chromatographic peaks are included in the  appendix.

        Ames Tests for mutagenicity on model aerosol products were also conducted.
   Products tested were  from toluene/NO , 1-heptene/NO , and a-pinene/NO  systems.
   None of the aerosol products from these systems showed mutagenic properties.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                        c  COSATI l-'icld/Group
   *Air pollution
   *Aerosols
   *Vapors
   *0rganic compounds
   *Chemical analysis
                                          13B
                                          07D
                                          07C
18 DISTRIBUTION STATEMENT

  RELEASE TO PUBLIC
              19 SECURITY CLASS (This Report/
                 UNCLASSIFIED
21 NO. OF PAGES

    81
                                              20 SECURITY CLASS (Tins page)

                                                 UNCLASSIFIED
                                                                        22. PRICE
EPA Form 2220-1 (9-73)

-------
1  REPORT NO
   EPA-600/3-78-039
4 TITLE ANDSUBTITLE

  VISIBILITY IN THE SOUTHWEST
  An Exploration of the  Historical Data Base
                                  TECHNICAL REFCRT DATA
                                           i lln> i  'iv hi/i>i i
                                                          3 RECIPIENT S ACCESSION-NO
                                PB-282-942
                                                          5 REPORT DATE
                                                            April  1973
                                                          G PERFORMING ORGANIZATION CC IE
7 AUTHORIS1
  J. Trijonis and Kung  Yuan
                                                            PERFORMING ORGANIZAT>ON Rf'ORTNO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Technology Service  Corporation
  2811 Wilshire Boulevard
  Santa Monica, California   90403
                                                          10 PROGRAM ELEMENT NO.

                                                             1AA603      AG-17 (FY-,77)
                                                          11 CONTRACT/GRANT NO
                                                             803896
12 SPONSORING AGENCY NAME AND ADDRESS
  Environmental  Sciences Research Laboratory - RTF,  NC
  Office of Research  and Development
  U.S. Environmental  Protection Agency
  Research Triangle Park,  North Carolina  27711	
                                                           13 TYPE OF REPORT AND PERIOD « fiVEREO
                                                             Tnt-Prim     3/77 -  ll/"7	
                                                          14 SPONSORING AGENCY CODE
                                                             EPA/600/09
15 SUPPLEMENTARY NOTES
  This research was  supported under EPA grant  803896 to Washington Univeristy,
  R.B. Husar, Principal  Investigator.
16 ABSTRACT
       The historical data base pertinent to visibility in the Southwest  is  analyzed.
  The data base  includes over 25 years of airport  visibility observations and  moie
  than 10 years  of  NASN particulate measurements.   The investigation covers  exis'.ing
  levels of visibility, long-term trends in visibility, and visibility/pollutant
  relationships.

       Although  still quite good, visibility in  the Southwest has deteriorated o-er
  the past two decades.  The haze levels in the  Southwest appear to be mostly  th.-
  result of secondary aerosols, especially sulfates.   These conclusions are  veri'ii?.d
  by decreases  in  sulfates and increases in visibility during the 1967-196S
  industry-wide  copper strike.
17.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                             b.lDENTIFIERS/OPEN ENDED TERMS
                                                                           COSATI field'Oroup
  * Air pollution
  * Aerosols
  * Sulfates
  * Visibility
                                                Southwest
    13B
    07D
    07B
18 DISTRIBUTION STATEMENT

   RELEASE TO PUBLIC
                                              19 SECURITY CLASS fTluv Ripart}
                                                 UNCLASSIFIED
21 NO OF PAGr?
 118
                                              20 SECURITY CLASS (Tins page)
                                                 UNCLASSIFIED  	
                                                                        22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REI ORT DATA
                            (Please read fnsiruciions on the reverse before completing)
1  REPORT NO
   EPA-600/3-78-043
            PB-280-559
                                                           3 RECIPIENT'S ACCESSION NO.
4 TITLE AND SUBTITLE


  DYNAMICS OF AUTOMOTIVE  SULFATE EMISSIONS
                                    5 REPORT DATE
                                      April 1978
                                    6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)

   S.H.  Suck, K. de Bower  and J.R. Brock
                                                           8. PERFORMING ORGANIZATION REPORT NO.
9 PERFORMING ORGANIZATION NAME AND ADDRESS
   Department of Chemical  Engineering
   University of Texas
   Austin, Texas  78712
                                    10. PROGRAM ELEMENT NO.
                                       1AA603  AE-09 (FY-77)
                                    11. CONTRACT/GRANT NO.

                                       Grant R803660
12. SPONSORING AGENCY NAME AND ADDRESS
   Environmental Sciences  Research Laboratory-RTF, NC
   Office of Research and  Development
   U.S.  Environmental Protection Agency
   Research Triangle Park,  North Carolina  27711
                                    13. TYPE OF REPORT AND PERIOD COVERED
                                       Interim  11/76 - 11/77
                                    14. SPONSORING AGENCY CODE
                                       EPA/600/09
15. SUPPLEMENTARY NOTES
16. ABSTRACT
        A preliminary  assessment of the potential environmental  impact  of automotive
   sulfuric acid  (or sulfate)  aerosol has been made by analyzing the aerosol dynamics.
   This analysis  leads to  the  prediction of ambient automotive sulfuric acid aerosol
   concentrations over and around a large, ten-lane highway  (48  m.  x 20 km.), some ten
   or so y°*rs hence,  when almost all cars in the United  States  will be fitted with
   catalytic converters.   The  attachment rate of fine automotive sulfuric acid
   aerosols to ambient aerosols is examined.  The dispersion and deposition of auto-
   motive sulfate are  modelled over the highway for "worst case" meteorology using
   K-theory.  The neutralizing effect of ambient ammonia  on  sulfuric acid concentra-
   tions around the highway is examined by a direct simulation procedure for dispersion
   calculations.  These calculations indicate that adverse environmental effects of
   automotive sulfuric acid emissions may be important under the stated conditions
   of this study.
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                       b.lDENTIFIERS/OPEN ENDED TERMS
c COSATI I icld/Group
   *Air pollution
   *Aerosols
   *Sulfuric acid
   *Sulfates
   *Automobiles
   *Exhaust emissions
 Catalytic converters
*Mathematica] models
 Highways
 Atmospheric diffusion
   13B
   07D
   07B
   13F
   21B
   07A
   04A
18. DISTRIBUTION STATEMENT

   RELEASE TO PUBLIC
                       19 SECURITY CLASS (This Report)
                           UNCLASSIFIED
21. NO. OF PAGES
        56
                                              20 SECURITY CLASS (Thispage)
                                                 UNCLASSIFIED
                                                                        22 PRICE
EPA Form 2220-1 (9-73)

-------
                                    TECHNICAL REP,
                              i. me icutl /tjurtit. nuns on tin-1
   REPORT NO
   EPA-600/3-78-045
 4 TITLE ANDSUBTITLE
                FIT DATA
                r»r he/on- iaiiii>lriiiifj
PB-281-014
   OXYGEN ISOTOPES IN ATMOSPHERIC SULFATES, SULFUR
   DIOXIDE, AND WATER VAPORS
   Field Measurements, July 1975	
                          5 REPORT DATE
                            April 1978
                          3 RECIPIENT'S ACCESSION NO.
                           PERFORMING ORGANIZATION CC'~E
   AUTHOR(S)
   B. Holt, M. Bouchard,  P.  Cunningham, A Kengelkemeir,
   E. Nielsen, S. Johnson, and  R.  Kumar
                         8 PERFORMING ORGANIZATION HE1 ORT NO
 9 PERFORMING ORGANIZATION NAME AND ADDRESS
   Argonne National Laboratory
   9700 South Cass Avenue
   Argonne, Illinois   60439
                          10 PROGRAM ELEMENT NO
                            1AA603  AH-01 (FY77)
                          11 CONTRACT/GRANT NO
                                                              IAG-D6-F024
  '. SPONSORING AGENCY NAME AND ADDRESS
   Environmental Sciences  Research Laboratory - RTP, NC
   Office of Research  and  Development
   U.S. Environmental  Protection Agency
                          13 TYPE OF REPORT AND PERIOD C:
                            Final  5/76 - 5/77
            'VERED
                          14 SPONSORING AGENCY CODE

                            EPA/600/09
 15 SUPPLEMENTARY NOTES
  e, ABSTI
        Oxygen isotope  ratios  were determined for atmospheric samples of sulfate
   aerosols, sulfur dioxide, and  water vapor collected  simultaneously during a si> -day
   period in July, 1975, at  St. Louis, MO; Auburn,  IL;  and  Glasgow,  IL.  The coll' :-
   tion sites were located about  100 km apart.

        Concerted variations in isotopic and concentration  results were found for  the
   three sites, demonstrating  an  apparent regional  imp/ict on  the quality and qunn1 Lty
   of particulate suifate in the  atmosphere.  At all  three  sites,  the oxygen-18
   enrichments in suspended  sulfates clearly varied inversely with sulfate concen
   tration.   This variation  suggests that sulfates  in cleaner air may have a different
   origin than sulfates  in more polluted air masses.  Samples collected during a
   period of local thunderstorm activity showed an  abrupt increase in the oxygen-!3
   composition of particulate  sulfate, but little effect on the isotopic composit •'-)n
   of ambient water vapor.

        The  lack of positive correlation between oxygen-18  variations in aerosol
   sulfate and oxygen-18 variations in water vapor  suggests that the aerosol sulf.i^e
   was not formed predominantly from the ambient water  in the air masses from whi^h it
   uac samlpd.
 7.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
   '••Air pollution
   *Sulfur dioxide
   ASulfates
   *Water vapur
   "Oxygen isotopes
    Chemic.il analysis
                                              l» IDENTIFIERS/OPEN ENDED TERMS
               St. Louis,  MO
               Auburn,  IL
               Glasgow,  IL
                                                                        c  COSATI I icld ''rou|i
   13B
   07B
   07D
   18B
 3 DISTRIBUTION STATEMENT

  RELEASE TO PUBLIC
            19 SECURITY CLASS (Tins Report)
               UNCLASSIFIED
21 NO OF PACT
  31
                                              3O SECURITY CLASS (tlits fia,<;ej

                                                 .UNCLASSIFIED
                                       22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL F' PORT DATA
                            (I'lca^c rriitl liiiliuctit'ii* on I  ;< i<;?< /ifjnit-1 tniiftli linv)
  REPORT NO
  EPA-600/3-78-048b
                                                           3 RECIPIENT'S ACCESSION-NO
           PB-279-409
4 TITLE AND SUBTITLE
   HOUSTON URBAN PLUME  STUDY - 1974
   Description and  Data
                                                           5 REPORT DATE
                                                             April 1978
                                   6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)

   James R. Brock
                                   8 PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
   The University of Texas
   Department of Chemical  Engineering
   Austin, Texas  78712
                                   10 PROGRAM ELEMENT NO
                                      1AA008
                                   11 CONTRACT/GRANT NO
                                                             R803660
 12 SPONSORING AGENCY NAME AND ADDRESS
   Environmental Sciences  Research Laboratory - RTF, NC
   Office of Research  and  Development
   U.S. Environmental  Protection Agency
   Research Triangle Park,  North Carolina  27711
                                   13 TYPE OF REPORT AND PERIOD COVERED
                                     Final
                                   14 SPONSORING AGENCY CODE
                                      FPA/600/09
 15. SUPPLEMENTARY NOTES
 16 ABSTRACT—

        The 1974 Houston  Urban Plume Study (HUPS) was undertaken as a preliminary
   investigation of  some  of the unresolved features of Houston's air pollution  pro-
   blem.  HUPS was intended specifically to gain limited information on  the  spatial
   and temporal distribution of air pollutants—particularly, primary and  secondary
   aerosols—in the  Houston area as an aid should a later intensive investigation  of
   aerosol character and  transport be needed.

        Aerial measurements were made of the principal pollutants  (S0_,  NO , 0_, CO,
   aerosol) of the Houston area.  Wind-field measurements were also made.  xThese
   data were used to estimate pollutant budgets.  Values for S0? and NO   (14 metric
   tons/hr and 40 metric  tons/hr, respectively) were reasonably comparable with values
   derived from emissions inventories of the Texas Air Control Board (13 and 24
   metric tons/hr, respectively).  On the basis of the limited sampling  period, the
   industrial area (east  of downtown Houston) apparently is the major contributor
   of primary air pollutants in the Houston area.  In the morning hours  above the
   mixed layer, relatively large ozone concentrations (max. 0.2 ppm)—almost
   certainly of photochemical—origin were found that correlated closely with light
   scattering aerosol,  thus indicating the existence above the mixed layer of strong
   secondary aerosol sources
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                                c COS AT I Field/Group
   *Air pollution
   *Aerosols
   *Sulfur dioxide
   ^Nitrogen oxides
   *0zone
    Plumes
   *Measurement
*Wind (meteorology)
 Airplanes
*Light scattering
Houston, TX
13B
07D
07B
23B
QIC
20F
13 DISTRIBUTION STATEMEIM1
   RELEASE TO PUBLIC
                      19
                                                21 NO OF Pf 3ES
                                                  260
                      20 SECURITY CLASS (Tinspage)
                         UNCLASSIFIED
                                                                        22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing)
 1 mW/3-78-075
                               PB-286-921
4. TITLE AND SUBTITLE
    VISI-BILITY IN THE NORTHEAST
    Long-Term Visibility Trends  and  Visibility/Pollutant
    Relationships	.	
                                                           3 RECIPIENT'S ACCESSION NO.
             5 REPORT DATE
               August  1978
             6. PERFORMING ORGANIZATION CODE
 7 AUTHOR(S)

    J.  Trijonis and Kung Yuan
                                                           8 PERFORMING ORGANIZATION REPORT NO
9. PERFORMING ORGANIZATION NAME AND ADDRESS

    Technology Service Corporation
    2811 Wilshire Boulevard
    Santa Monica, California  90403
             10. PROGRAM ELEMENT NO.

               1AA603     AG-17 fFY-771
             11. CONTRACT/GRANT NO

               803896
 12. SPONSORING AGENCY NAME AND ADDRESS
    Environmental Sciences Research  Laboratory - RTF, NC
    Office of Research and Development
    U.S. Environmental Protection Agency
    Research Triangle Park. North Carolina  27711	
             13. TYPE OF REPORT AND PERIOD COVERED
               Interim    JO/77 -  4/78	
             14. SPONSORING AGENCY CODE
               EPA/600/09
 15. SUPPLEMENTARY" NOTES
    This research was supported under  EPA grant 803896 to Washington University,
    R.B. Husar, Principal Investigator.
 16. ABSTRACT
      The historical data basu  p.'itin'i I    ubscrv.-itions and
 more than 10 years of NASN particular ".tu^urtmoTils.  The investigation covers
 existing visibility levels,  long-term trends  in visibility, and visibility/pollutant
 relationships.

      Visibility in the Northeast  is  rather poor, median visual range being on the ordei
 of 10 miles.  Visibility is  not now  substantially better in nonurban areas than in
 metropolitan areas of the Northeast.   From the middle '1950's to the  early 1970's,
 visibility exhibited only slight  trends  in large metropolitan areas  but decreased on
 i lu' order*of 10 to 40% at suburban and nonurban locations.  Over  the same period,
 \"'..uil range declined remarkably  during  the third calendar quarter relative to other
 siMsuns, making the summer now the worst season for visibility.   The decrease in
 visibility during the summer was  especially notable at suburban and  nonurban locations,
 where atmospheric extinction apparently  increased on the order of 50 to 150% during
 the third calendar quarter.

      Regression models based on daily variations in visibility and pollutant concentra
 tions indicate that sulfate  aerosol  is the single major contributor  to  haze in the
 Northeast.   Sulfates apparently account  for approximately 50% of  total  extinction.
 7.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                             b IDENTIFIERS/OPEN ENDED TERMS
                             COSATI Field/Group
    *Aii* pollution
    *Aerosols
    *Sulfates
    *Visibility
    *Trends
    *Haze
    *Mathematical models
     Northeast
 13B
 07D
 07B
 12A
 04 B
18 DISTRIBUTION STATEMENT

    RELEASE. TO PUBLIC
19 SECURITY CLASS (Thu Report)
    UNCLASSIFIED
                           21
NO OF PAGES
 94
                                              20 SECURITY CLASS (ThU page)
                                                  UNCLASSIFIED
                                                                        22. PRICE
EPA Form 2220-1 (9-73)

-------
 I
       TECHNICAL REPCHT DATA
(Please read fuuriictioiis on the rc\ • rsc before completing)
 1  REPORT NO

   EPA-600/3-79-001a
    PB-290-507
                              3 RECIPIENT'S ACCESSION-NO.
 4 TITLE ANDSUBTITLE
  MODELING  OF  SIMULATED PHOTOCHEMICAL SMOG WITH  KINETIC
  MECHANISMS    Volume 1.  Interim Report
                              5 REPORT DATE
                                January 1979
                              6. PERFORMING ORGANIZATION CODE
 7 AUTHOR(S)
  G.Z. Whitten,  H.  Hogo, M.J. Meldgin, J.P. Killus,
  and P. J.  Bekowies
                              8. PERFORMING ORGANIZATION REPORT NO


                                   EF78-121A
 9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Systems Applications, Incorporated
  950 Northgate  Drive
  San Rafael,  California  94903
                               10. PROGRAM ELEMENT NO

                                1AA603   AC-19 (FY-78)
                               11. CONTRACT/GRANT NO

                                Contract No. 68-02-2428
 12. SPONSORING AGENCY NAME AND ADDRESS
  Environmental  Sciences Research Laboratory-RTP, NC
  Office of  Research and Development
  U.S. Environmental  Protection'Agency
  Research Triangle Park. N.C.  27711	
                               13. TYPE OF REPORT AND PERIOD COVERED
                                Interim  7/76-7/78
                              14. SPONSORING AGENCY CODE
                                 EPA/600/09
 15. SUPPLEMENTARY NOTES
   Volume'2.  Appendix   EPA-600/3-79-001b
 16. ABSTRACT
       Computer modeling of smog chamber data is discussed in three parts.  First,
  a series of detailed chemical  mechanisms were developed to describe the photo-
  chemical formation  of ozone from nitrogen oxides and the following organic
  compounds  (alone  and in various combinations):  formaldehyde, acetaldehyde,
  ethylene,  propylene, butane, 1-butene, trans-2-butene, and 2,3-dimethylbutane.
  Second, a  generalized kinetic  scheme intended for use in models simulating
  the formation of  ozone in urban atmospheres was refined.  The generalized
  mechanism  includes  a condensed version of the detailed mechanisms developed
  in the first part plus a semi-empirical scheme to describe the oxidation of
  aromatic hydrocarbons.  Third, the effects of smog chambers on ozone formation
  were examined.  For this part  of the study, similar experiments using nitrogen
  oxides and propylene in eight  different smog chambers were simulated using
  the detailed propylene mechanism.  The main chamber effects identified thus
  far are apparently  due to nitrogen oxides degassing from the walls during
  experiments and differences between chambers in the spectral distribution
  of ultraviolet irradiation.
    •   Volume 1 contains all  textual  material.  Volume 2 contains graphs of measured and
  Simulated  POllUtant. mnrpntratinns fnr many cmng rhamher a
 7.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
     Air pollution
     Reaction kinetics
     Photochemical reactions
     Test chambers
     Mathematical models
     Computerized simulation
                                              b IDENTIFIERS/OPEN ENDED TERMS  C. COSATI Field/Croup
                                             13B
                                             07D
                                             07E
                                             14B
                                             12A
                                             09B
 8 DISTRIBUTION STATEMENT
 RELEASE  TO PUBLIC
                                              19 SECURITY CLASS (This Report}
                                               UNCLASSIFIED
                                           21. NO. OF PAGES
                                               332
                                                            (Tins page)
                                                                        22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPORT DATA
                            (Please read Inunctions on the re> i rse before completing)
 1 REPORT NO
   EPA-600/3-79-001b
                                PB-290-508
                                                           3. RECIPIENT'S ACCESSION-NO.
 4. TITLE AND SUBTITLE
  MODELING OF  SIMULATED PHOTOCHEMICAL SMOG WITH KINETIC
  MECHANISMS    Volume 2.   Interim Report Appendix
                                                      5. REPORT DATE

                                                        January 1979
                                                      6. PERFORMING ORGANIZATION CODE
  , AUTHOR(S)
  G. Z. Whitten,  H.  Hogo,  M.J.  Meldgin, J.P. Killus,
  and P.J. Bekowies
                                                      8. PERFORMING ORGANIZATION REPORT NO

                                                           EF78-121B
          IG ORGAFi
                   ATION NAME AND ADDRESS
  Systems Applications,  Incorporated
  950 Northgate  Drive
  San Rafael, California   94903
                                                      10. PROGRAM ELEMENT NO.
                                                         -k.

                                                        lAAfin.3   Af.-TQ /FY-78)
                                                      11. CONTRACT/GRANT NO.
                                                            Contract No.  68-02-2428
 12 SPONSORING AGENCY NAME AND ADDRESS
  Environmental  Sciences  Research Laboratory-RTP, NC
  Office of Research  and  Development
  U.S. Environmental  Protection-Agency
  Research Triangle Park,  N.C.   27711
                                                      13. TVPE OF REPORT AND PERIOD COVERED
                                                        Interim   7/76-7/78
                                                      14. SPONSORING AGENCY CODE

                                                         EPA/600/09
  5. SUPPLEMENTARY NOTES
  Volume"1.   Interim Report   EPA-600/3-79-001a
       Computer modeling  of  smog chamber data is discu-ssed in  three  parts.   First,
  a series of detailed  chemical  mechanisms were developed to describe  the photo-
  chemical formation  of ozone  from nitrogen oxides and the following organic
  compounds (alone and  in various combinations):  formaldehyde, acetaldehyde,
  ethylene, propylene,  butane,  1-butene, trans-2-butene, and 2,3-dimethylbutane.
  Second,' a generalized kinetic  scheme intended for use in models simulating
  the formation of ozone  in  urban atmospheres was refined.  The generalized
  mechanism includes  a  condensed version of the detailed mechanisms  developed
  in the first part plus  a semi-empirical  scheme to describe the oxidation  of
  aromatic hydrocarbons.   Third, the effects of smog chambers  on ozone formation
  were examined.  For this part  of the study, similar experiments using nitrogen
  oxides and propylene  in  eight  different smog chambers were simulated using
  the detailed propylene  mechanism.   The main chamber effects  identified thus
  far are apparently  due  to  nitrogen oxides degassing from the walls during
  experiments and differences  between chambers in the spectral distribution
  of ultraviolet irradiation.
       Volume 1 contains  all textual  material.  Volume 2 contains graphs of measured anc
  simulated pollutant concentrations for many smog chamber experiments.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
Air pollution
Reaction kinetics
Photochemical reactions
Test chambers
Mathematical models
Computerized simulation
                                             b IDENTIFIERS/OPEN ENDED TERMS
                                                                        c. COSATI Field/Group
                                                                          13B  .
                                                                          07D
                                                                          07E
                                                                          14B
                                                                          12A
                                                                          09B
  . DISTRIBUTION STATEMENT

  RELEASE TO PUBLIC
                                         19 SECURITY CLASS (Tins Report!
                                          UNCLASSIFIED
21. NO. OF PAGES

     414
                                             20 SECURITY CLASS (This page)
                                               UNCLASSIFIED
                                                                   22. PRICE
EPA Form 2220-1 (9-73)

-------
                                    TECHNICAL RETORT DATA
                             (I'li'iHc read laajiicnons on Ilic rci ci w bcjoic conij'lctiiif)
 1  REPORT NO
   EPA-600/3-79-006
PB-290-859
 4 TITLE AND SUBTITLE
   LABORATORY INVESTIGATION  OF THE PHOTOOXIDATION AND
   CATALYTIC OXIDATION OF  SO,,
                         6 PERFORMING ORGANIZATION CODE
                         3 RECIPIENT'S ACCESSION-NO
                         5 REPORT DATE
                            January 1979
 7 AUTHORIS)
    R.J.  Anderson, R.J. Pilie,  E.J. Mack, W.C. Kocmond
                         8 PERFORMING ORGANIZATION REPORT NO
                          NA-5781-M-1
   PERFORMING ORGANIZATION NAME AND ADDRESS
    Calspan Corporation
    Advances Technology  Center
    4455 Cenesee Street
    Buffalo, NY  14225
                         10 PROGRAM ELEMENT NO
                             1AA603   AC-13  FY77
                         11 CONTRACT/GRANT NO
                          68-02-1785
 12 SPONSORING AGENCY NAME AND ADDRESS
   Environmental Sciences  Research Laboratory - RTF,  NC
   Office of Research and  Development
   U.S.  Environmental Protection Agency
   Research Triangle Park,  North Carolina  27711	
                         13. TYPE OF REPORT AND PERIOD COVERED
                          Final
                         14 SPONSORING AGENCY CODE

                          EPA/600/09
 15 SUPPLEMENTARY NOTES
 16 ABSTRACT
         The photooxidation of S02 in irradiated  auto  exhaust + S02 systems, the
    catalytic oxidatioii  of  S02 in the solution droplets  of hazes, clouds and fogs
    containing several concentrations of heavy metals  (Hn+2 and Fe+3), and the
    oxidation of S02  in  irradiated hazes and  fogs containing only trace quantities of
    heavy metals were studied in a 590 m  indoor  smog  chamber.  For the irradiated
    auto exhaust + S02 systems, S02 oxidation rates  as high as 5% hr~l were observed.
    Primary particulates from auto exhaust produced  no discernible effect on S02
    oxidation.  Catalytic oxidation of S02 in fogs and hazes was significant under
    certain conditions,  with as much as 6% of the available S02 being oxidized in a
    30-minute period.  No synergistic effect  on the  rate of S02 oxidation was observed
    from the simultaneous presence of irradiation and  a  fog or haze.
                                 KEY WORDS AND DOCUMENT ANALYSIS
                   DESCRIPTORS
    AAir pollution
    *Sulfur dioxide
    *Aerosols
    ^Photochemical reactions
    *C.iL;i lysis
    *Sulfates
    *Test chambers
                                               L) IDENTIFIERS/OPEN ENDED TERMS
                                         COS ATI I lclil/Croii|i
                                        ~]~3B
                                          07B
                                          07D
                                          07F.
 18 DISTRIBUTION STATEMENT
    RELEASE TO PUBLIC
                                               19 SECURITY CLASS (rins Report)
                                                   UNCLASSIFIED
                                       21 NO OF PAGES
                                          88
                                               20 SECURITY CLASS (Tinspascj
                                                   UNCLASSIFIED
                                                                         22 PRICE
•EPA Form 2220-1 (9-73)

-------
                                    TECHNICAL FT  'ORT DATA
                             /'/., i. '.W Ilium lii'in in; ;'  •• i. ;\,- '« f.vi-
     i r NO
EPA-600/4-78-020
                                PB-279-706
 J TITLE AND SUBTITLE"

   REGIONAL AIR POLLUTION STUDY
   Fugitive Dust Survey and Inventory
   AUTHOR(S)              ~

   Robert W.  Griscorn, Edward 0. Nelson,  and
   Fred  E.  Littmann
 9 PERFORMING ORGANIZATION NAME AND ADDRESS
   Rockwell  International Air Monitoring Center
   11640  Administration Drive
   Creve  Coeur,  MO  63141
 12 SPONSORING AGENCY NAME AND ADDRESS
   Environmental  Sciences Research Laboratory-RTP,  NC
   Office of  Research and Development
   U. S. Environmental  Protection Agency
   Research Triangle Park.  North Carolina  27711
              3 RECH'ILN r ••, ACCESSlOr»NO


              5 RFPOR1  DATE

                  APRIL 1978
              G PbHI OhMINL, uRr;j\NI7A1 ION COUh
              8 PEKI ORMINU ORGANIZATION RfPORl NO
              10 PROGRAM CLEMENT NO~

              _LAA6_0_3_
              tl CONTRACT
                rONTRACT/GRANT NO

               68-02-2093
               Task  Order 124
              13 T.YPE OF REPORT AND PERIOD COVERED
               Final
              14 SPONSORING AGENCY CODE
               EPA/600/09
 75 SUPPLEMENTARY NOTES
                I-  E   R?9lonal  A}r Pollution Study,  ten monitoring stations were
                high  volume samplers and automatic dichotomous samplers to measure
 concentrations  of atmospheric aerosols.  In addition, two of the S?  LoSis City
 monitoring  sites  were  used for special aerosol studies.   Because of the strong
       1  tlnfluence °f nearby 9™^-^! fug1tlve  dust  soSrcJ on ierosol Sasure-
          S  J"™*5 Were  ?de within a radius of one mile of each site to asses
       thp f 11    CeS'  and a" emlssions ^ventory  of these sources was calculated
 caved strJt    ™??ATCe "te9orles:  clea^d areas,  construction, playgrounds
                 raioad "ght-of-way and yards, and  agricultural  tilling and wind

                             *9™ ^ "Ch Slte ™ ^^                  "
                                KT.Y WOHOS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
 * Air  pollution
 * Aerosols
 * Particles
 * Measurement
 * Field  tests
 3 DISTRIBUTION STATEMENT
   RELEASE  TO PUBLIC
EPA Form 2220-1 (9-73)
I' IDENTIFIERS/OPEN ENDED TERMS

 St. Louis, MO
                                              10 SECURITY CLASS (Ilm Ri,initJ

                                             __UNCLASSI£I£H.
                                              20 SECURITY CLASS (llu\pavf)

                                                UNCLASSIFIED
                                                                        «.  COSATI I
                                                                          13B
                                                                          07D
                                                                          14B
                           21 NO OF p/ QES
                              218
                           22 PRICE

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing)
1  REPORT NO.
  EPA-600/4-78-041
                             2.
                                 PB-287-101
                                                          3. RECIPIENT'S ACCESSION NO
                      STRUCTURE AND TURBULENT DIFFUSION
 AROUND A THREE-DIMENSIONAL HILL
 Fluid Modeling  Study on Effects of Stratification
 Part I. Flow  Structure	
             5 REPORT DATE

                      1978
   July
             6. PERFORMING ORGANIZATION CODE
_-—-—• ~
7 AUTHOR(S)

 J.C.R. Hunt1,  W.H.  Snyder2, R.E. Lawson, Jr.
             8 PERFORMING ORGANIZATION REPORT NO,
                                                            Fluid Modeling Report No. 4
9 PERFORMING ORGANIZATION NAME AND ADDRESS

 Environmental  Sciences Research Laboratory
 Office  of Research and Development
 U.S. Environmental Protection Agency
 Research  Triangle Park. N.C.  27711	
             10 PROGRAM ELEMENT NO

                1AA603  AB-20 (FY-78)
             11 CONTRACT/GRANT NO.
12 SPONSORING AGENCY NAME AND ADDRESS
 Environmental  Sciences Research Laboratory
 Office  of Research and Development
 U.S.  Environmental Protection Agency
 Research Triangle Park. N.C.  27711	
—RTP, NC
13. TYPE OF REPORT AND PERIOD COVERED
 In-house   4/1/77  -  3/31/78
             14. SPONSORING AGENCY CODE
               EPA/600/09
15 SUPPLEMENTARY NOTES
  1.  University of Cambridge, England.   2. On  assignment  from  National  Oceanic  and
  Atmospheric Administration, Dept.  of  Commerce.   3.  Northrop  Services, Inc.
16 ABSTRACT
   This  research program was initiated with  the  overall  objective  of gaining  understand-
ing  of  the flow and diffusion of  pollutants in  complex  terrain  under both neutral  and
stably  stratified conditions.  This  report  covers  the first  phase of the  project;  it de-
scribes the flow structure observed  over  a  bell  shaped  hill  (polynomial  in cross  sectior
through neutral wind tunnel studies  and stably  stratified towing  tank studies.   It
verifies and establishes the limits  of applicability of Drazin's  theory  for  flow  over
three-dimensional hills under conditions  of small  Froude number.   At larger  Froude
number  a theory is developed, and largely verified,  to  classify the types of lee  wave
patterns and separated flow regions  and to  predict the  conditions under which they will
be formed.  Flow visualization techniques are used extensively  in obtaining  both
qualitative and quantitative information  on the flow structure  around the hill.   Repre-
sentative photographs of dye tracers, potassium permanganate, dye streaks, shadowgraphs,
surface dye smears, and hydrogen  bubble patterns are included.  While emphasis  centered
on obtaining basic understanding  of  flow  around complex terrain,  the results are  of
immediate applicability by air pollution  control agencies.   In  particular, the  location
of the  surface impingement point  from an  upwind pollutant source  can be  identified under
a wide  range of atmospheric conditions.   Part II,  to be printed as a separate report,
will describe the concentration field over  the  hill  resulting from plumes released from
upwind  stacks and will further quantify the results  obtained in Part I.
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lDENTIFIERS/OPEN ENDED TERMS
                           c  COSATI Held/Group
     Air pollution
     Wind(meteorology)
     Wind tunnel  models
     Hills
     Atmospheric  diffusion
     Stratification
     Flow distribution
                                13B
                                04B
                                14B
                                08F
                                04A
                                20D
18 DISTRIBUTION STATEMENT
         RELEASE TO PUBLIC
                                              19 SECURITY CLASS (This Report)

                                                 UNCLASSIFIED	
                           21 NO OF PAGES

                                96
                                              20 SECURITY CLASS (Thupage)

                                                 UNCLASSIFIED
                                                                        22 PRICE
EPA Form 2220-1 (Rev. 4-77)   PREVIOUS EDITION is OBSOLETE

-------
                                   TECHNICAL REPORT DATA
                            (PUase read Instructions en the n?i srse before temple tingl
 REPORT NO
  EPA-600/4-78-042
                                                            3 RECIPIENT'S ACCESSION NO.
PB-290-921	
 . TITLE AND SUBTITLE
 REGIONAL  AIR POLLUTION STUDY
 Point Source Methodology and  Emission Inventory
                          5 REPORT DATE
                            July  1978
                          6. PERFORMING ORGANIZATION CODE
 AUTHOR(S)
 F.E.  Littman
                                                            8. PERFORMING ORGANIZATION REPORT NO.
 PERFORMING ORGANIZATION NAME AND ADDRESS
 Rocf(well  International
 Air Monitoring Center
 11640  Administration Drive
 Creve  Coeur, MO  63141
 2. SPONSORING AGENCY NAME AND ADDRESS
 Environmental Sciences  Research Laboratory  -  RTP, NC
 Office  of Research and  Development
 U.S.  Environmental Protection Agency
 Research Triangle Park,  NC  27711
                          10 PROGRAM ELEMENT NO.
                            1AA603  AA-07 (FY-77)
                          11. CONTRACT/GRANT NO
                            68-02-2093
                            Task  Order 108A
                          13. TYPE OF REPORT AND PERIOD COVERED
                             Final
                          14. SPONSORING AGENCY CODE
                             EPA/600/09
IS. SUPPLEMENTARY NOTES
16. ABSTRACT

       The development  of the point source  emission data inventory for the Regional
  Air  Pollution Study at St.  Louis is discussed.   To meet the  unusual  requirements
  of this study, which  specified the acquisition  of hourly, measured emission data
  for  the St. Louis Air Quality Control Region for a period of two years, a unique
  methodology was developed and put into practice.  The result is  a data base con-
  taining over 20 million pieces of information in a readily accessible form.
17
                                KEY WORDS £NO DOCUMENT ANALYSIS
                  DESCRIPTORS
  *Air pollution
  *Emission
  *Environmental  surveys
  *Sources
                                               (• IDENTIFIERS/OPEN ENDED TERMS
              St.  Louis, MO
                                           COSATI I Idd/Gmup
  13B
  050
18 DISTRIBUTION STATEMENT
  RELEASE TO  PUBLIC
             19 SECURITY CLASS (This Report I

                IINHASSIFIED
21. NO OF PAGES
   160
             20 SECURITY CLASS (Thispage)
                UNCLASSIFIED
                                                                           22 PRICE
EPA Form 2220-1 (Rev. 4-77)   PREVIOUS EDITION is otisc i.r T E

-------
                                   TECHNICAL REPORT DATA
                            (flease read Inunctions on the rc\ cnc before completing)
1 REPORT NO.
  EPA-600/4-78-044
PB-289-451
                                                           J RECIPIENT'S ACCESSION-NO.
4 TITLE AND SUBTITLE

  A PILOT  STUDY ON DISPERSION  NEAR ROADWAYS
                          5 REPORT DATE
                             August 197P
                                                           6 PERFORMING ORGANIZATION CODE
7. AUTHORIS)

  William B.  Petersen
                                                           8. PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
                                                           10. PROGRAM ELEMENT NO

                                                              1AA603   AB26  (FY-78)
   (same as block  12)
                                                           17. CONTRACT/GRANT NO.
 12. SPONSORING AGENCY NAME AND ADDRESS
   Environmental Sciences Research  Laboratory-  RTP,  NC
   Office  of Research and Development
   U. S. Environmental Protection Agency
   Research Triangle Park, NC   27711
                           13. TYPE OF REPORT AND PERIOD COVERED
                             In-House	
                           14. SPONSORING AGENCY CODE
                             EPA/600/09
15. SUPPLEMENTARY NOTES
 16. ABSTRACT
      High  frequency wind fluctuation data were used to estimate  the  dispersion
 near roadways.   The standard deviations of the wind direction and  the  elevation
 angle were computed for six averaging times.  The EPA HIWAY model was modified
 to use  these fluctuation statistics directly to estimate dispersion.   The data
 from the General Motors Sulfate Dispersion Experiment were used  in this study.
 In particular,  the data used in this pilot study were three half-hour  periods when
 the winds  were nearly parallel  with the test track.  Results from  analysis show
 that model performance was improved for parallel wind conditions when  the fluctuation
 statistics of the wind were used to estimate dispersion.  The results  also show
 that model estimates are most  sensitive to the vertical dispersion parameter.  Indeed,
 concentrations seem to be insensitive to the horizontal dispersion parameter.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
 *Air pollution
 *Wind (meteorology)
 *Atmospheric diffusion
 *Roads
 *Mathematical models
             b.lDENTIFIERS/OPEN ENDED TERMS  C. COSATI I'lcld/Group
                                           13B
                                           04B
                                           04A
                                           13B
                                           12A
18 DISTRIBUTION STATEMENT
 RELEASE  TO PUBLIC
                                              19. SECURITY CLASS (This Report)

                                                UNCLASSIFIED	
                                        21 *'O OF PAGFS
                                             31
             20 SECURITY CLASS (Tins page)
                UNCLASSIFIED
                                                                         22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing)
 i REPORT NO.
  EPA-600/4-78-049
                             2.
                              PB-289-806
                                                           3. RECIPIENT'S ACCESSION-NO.
4. TITLE AND SUBTITLE
   SELECT RESEARCH GROUP IN AIR POLLUTION METEOROLOGY

   Third Progress Report
                                                       5 REPORT DATE
                                                        August  1978
                                                       6. PERFORMING ORGANIZATION CODE
7. AUTHORISI
   R. Anthes, A. Blackadar,  R.  Kabel, J. Lumley,
   H. Tennekes and D. Thompson
                                                           8. PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AND ADDRESS
   Dept. of Meteorology  and  Center for Air Environment
   Studies.
   The Pennsylvania State  University
   University Park, Pennsylvania  16802
                                                       10. PROGRAM ELEMENT NO.
                                                         1AA603  AB-02   (FY-78)
                                                       11. CONTRACT/GRANT NO.
                                                         R-800297
 12. SPONSORING AGENCY NAME AND ADDRESS
   Environmental  Sciences Research Laboratory - RTF,  NC
   Office of Research and -Development
   U.S. Environmental Protection Agency
   Research Triangle  Park,  North Carolina   27711	
                                                       13. TYPE OF REPORT AND PERIOD COVERED
                                                         Interim   10/74  -  10/76
                                                       14. SPONSORING AGENCY CODE
                                                         EPA/600/09
 15. SUPPLEMENTARY NOTES
16. ABSTRACT
        Six  individual investigators, who have  conducted different but  related meteor-
   ological  research,  present in-depth  technical reviews of their work.   Prime con-
   clusions  are that (1) a scale analysis shows that different models are necessary
   for meteorological  processes on urban, regional and global scales;  (2) for high
   resolution models of the nocturnal planetary boundary layer, K theory models are
   very efficient,  realistic and useful;  (3)  the mixing height has a significant
   effect  on climatology models; (4) second moment closure methods are  useful for
   convective situations, properly testing  counter gradient fluxes;  (5) natural
   sources and pollutants acting at  the surface of the earth are important for air
   quality simulation models; and  (6) a combination of conventional micrometeorological
   and acoustic sounder techniques are  sufficient for verifying locally applied inver-
   sion use, box, and regional scale modles,  and urban and regional models require a
   variety of in situ and remote observation.
17.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lDENTIFIERS/OPEN ENDED TERMS  C.  COSATI Ficld/GlOUp
*  Air pollution
* .Meteorology
*  Mathematical models
*  Boundary  layer
                                                                          13B
                                                                          04B
                                                                          04A
                                                                          12A
                                                                          20D
18 DISTRIBUTION STATEMENT

    RELEASE TO PUBLIC
                                          19. SECURITY CLASS (ThisReport)
                                               UNCLASSIFIED	
                                                                         21. N
2°32°F
                                              20 SECURITY CLASS (Thispage)
                                                   UNCLASSIFIED
                                                                         22. PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL nEFPr1, r DATA
                            (PLasc read lastnu. dims on ilic rcn'ist bi-
U BfPAR-off6V4-78-050
                             2.
PB-287-473
                                                           3 RECIPIENT'S ACCESSION"NO.
4 TITLE AND SUBTITLE

   TURBULENCE MODELING APPLIED TO BUOYANT PLUH'-S
                         5 REPORT DATE
                           August 1978
                                                           6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)

    M.L.  Teske, W.S. Lewellen,  and H.S. Segur
                                                           8. PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AND ADDRESS
    Aeronautical Research Associates of Princeton,  Inc.
    50 Washington Road
    Princeton, New Jersey  08540
12. SPONSORING AGENCY NAME AND ADDRESS
    Environmental Sciences Research Laboratory  -  RTF,  NC
    Office of Research  and Development
    U.S. Environmental  Protection Agency
    Research Triangle Park, North Carolina   27711	
                          10. PROGRAM ELEMENT NO.
                           1AA601  CA-31  (FY-78)
                          11. CONTRACT/GRANT NO.

                           68-02-2285
                          13 TYPE OF REPORT AND PERIOD COVERED
                          Interim6/76  - 6/77	
                          14. SPONSORING AGENCY CODE
                           EPA/600/09
15 SUPPLEMENTARYWOTES
16. ABSTRACT           '•           ]
         A viable  computer model was developed  that is based on second-order closure
    of the turbulent correlation equations  for  predicting the fate of nonchemically
    reacting  contaminants released in  the atmcr.nheric boundary layer.  The invariant
    turbulence  model discussed in previous  repotts has been extended to compute  the
    development of buoyant plumes.  Nu.rrrical  program capability has been extended by
    improving the  speed and accuracy of  the two-dimensional unsteady turbulent flow
    calculation.   Plume calculations ore. nade  for buoyant plumes rising into a stable
    quiescent atmosphere and stable, neutral,  and unstable moving atmospheres.   An
    examination of the application of  an integral .ipproach to our turbulent boundary
    layer model is also included.
17.
                                KEY WORDS AND DOCUMENl ANALYSIS
                  DESCRIPTORS
 *Air  pollution
 *Meteorology
 *Turbulence
 *Turbulent'flow
 '"'Atmospheric diffusion
 *Mathematical Models
                                              b IDENIIFIERS/OPEN ENDED TERMS
                                                                        c.  COSATI Field/Group
                                           13B
                                           04B
                                           ?OD
                                           OAA
                                           12A
18 DISTRIBUTION STATEMENT

     RELEASE TO PUBLIC
             19 SECURITY CLASS (Tins Report)
                  UNCLASSIFIED
                                                                         21. NO OF PAGES
                                              20 SECURITY CLASS (Thispage!
                                                   UNCLASSIFIED
                                                                         22. PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the rcicrse before completing)
. REPORT NO

 EPA-600/4-79-001
                                                            3. RECIPIENT'S ACCESSION-NO.
 TITLE AND SUBTITLE
    REGIONAL AIR POLLUTION  STUDY
    Lambert Field Graphical  Weather Summary
                          5. REPORT DATE
                            January  1979
                          6«ttRFORMING ORGANIZATION CODE
 AUTHOR(S)

    Robert B.  Jurgens and William Ted Smith**
                                                            8. PERFORMING ORGANIZATION REPORT MO.
 PERFORMING ORG -\NIZATION NAME AND ADDRESS
                          10. PROGRAM ELEMENT NO.
                              1AA603  AA-49 (FY-78)
                           (Same as 12)
                                                            11. CONTRACT/GRANT NO
 2. SPONSORING AGENCY NAME AND ADDRESS
    Environmental  Sciences  Research Laboratory - RTP,  NC
    Office of  Research and  Development
    U. S. Environmental  Protection Agency
    Research Triangle Park.  NC  27711	
                          13. TYPE OF REPORT AND PERIOD COVERED

                             Tn-hnii«;p
                          14. SPONSORING AGENCY CODE
                             EPA/600/09
 6. SUPPLEMENTARY NOTES

 ** Potomac  Research,  Inc.
    Research Triangle  Park.
27711
16. ABSTRACT
         Three-hour meteorological observations from Lambert Field,  St. Louis,
    Missouri  are presented in graphical  format for  the three-year period
    July 1974 to June  1977.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                               b.lDENTIFIERS/OPEN ENDED TERMS
                                           COSATI I Icld/Group
          Air Pollution
          Meteorological  data
          Graphic Methods
St.
                              Mo.
13B
04B
12A
18. DISTRIBUTION STATEMENT
          RELEASE  TO PUBLIC
             19 SECURITY CLASS (Thu Report)

                 UNCLASSIFIED
                       21 NO OF PAGES
                           43
             20 SECURITY CLASS (This page)
                  UNCLASSIFIED
                                                                           22. PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the re\ i.rsc before completing)
1  REPORT NO
  EPA-600/4-79-002
PB-292-489
                                                          3 RECIPIENT'S ACCESSION-NO
4 TITLE AND SUBTITLE
  ANALYSIS OF ENSEMBLE  AVERAGED CONCENTRATIONS AND
  FLUXES IN A TRACER  PUFF
                                                          5 REPORT DATE
                                                            January 1979
                          6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S)

  Main R. Hutcheson
                                                          8. PERFORMING ORGANIZATION REPORT NO
9. PERFORMING ORG '\NIZATION NAME AND ADDRESS
  School of Meteorology
  University of Oklahoma
  Norman, Oklahoma   73019
                                                           10. PROGRAM ELEMENT NO.
                                                             IAA603  AB-13 (FY-78)
                           11 CONTRACT/GRANT NO.

                             Grant 804507
12. SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences  Research Laboratory - RTP,  NC
  Office of Research  and  Development
  U.S. Environmental  Protection Agency
  Research Triangle Park,  NC  27711
                           13. TYPE OF REPORT AND PERIOD COVERED
                             Final      	
                           14. SPONSORING AGENCY CODE
                             EPA/600/09
15. SUPPLEMENTARY NOTES
16. ABSTRACT
       Ensemble averaged fluxes and concentrations  in a  tracer  puff diffusing in the
  atmospheric surface  layer were analyzed.  The analysis  used radiation data published
  by the Battelle Memorial  Institute.  Fluxes that  satisfy  the  diffusion equation for
  a Gaussian puff with an arbitrary diffusion rate  were  obtained  from the gradient
  transfer hypothesis, using the proper diffusivities.   These fluxes were used as
  estimates of the  ensemble averaged fluxes in the  surface  layer.
       The radiation data,  however, were too sparse to use  alone  in analyzing the
  tracer concentrations.   Therefore, the data were  combined with  a  modified Gaussian
  distribution in a variational technique to obtain concentration values.   Since the
  ensemble averaged concentration distribution was  more  nearly  normal  than the distri-
  bution in an individual  puff, the concentration estimates were  obtained from a model
  using a Gaussian  distribution in the horizontal,  which  constrained the estimates as
  close to the analyzed concentrations as possible.
       The concentration and flux estimates were combined with  the  diffusion equation
  in a variational  technique.   The analyzed fluxes  and concentrations obtained were
  close to the estimates and satisfied the diffusion equation.  The values are assumed
  to be the true ensemble averaged concentrations and fluxes for  the puffs examined.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
              b.lDENTIFIERS/OPEN ENDED TERMS  C. COSATI Field/Croup
  Air pollution
  Mathematical data
 *Atmospheric diffusion
 *Flux density
  Applications of mathematics
                                                13B
                                                04B
                                                04A
                                                12A
18. DISTRIBUTION STATEMENT
                                              19. SECURITY
                                                              i« Report)
              RELEASE  TO PUBLIC
                                        21. NO OF PAGES

                                            111
                                              20 SECURITY CLASS (This pagef

                                              	IINfl ASSTFTFD
                                                                        22. PRICE
EPA Form 2?ZD-1 (9-73)

-------
                                  TECHNICAL REPORT DATA -
                           fPlcatc rcatl /uUfiiclioiis on llie r> \ i-isc before toiii/>lctnix)
1  REPORT NO
  EPA-600/4-79-003
                                  PB-290-660
4 TITLE ANDSUBTITLE
 REGIONAL AIR POLLUTION STUDY
 High Volume Filter Measurements of  Suspended Particulate
 Matter
                                                          3 RECIPIENT'S ACCESSION NO
                                                          5 REPORT DATE
                                                            January.. 19.79
                                                          6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
 E.  Nelson
                                                          8. PERFORMING ORGANIZATION REPORT NO.
9 PERFORMING ORGANIZATION NAME AND ADDRESS
 Rockwell International
 Environmental Monitoring & Services  Center
 11640. Administration  Drive
 Creve Coeur, MO  63141
                                                          10. PROGRAM ELEMEN1

                                                           1AA603
                                                                           NO
                                                          11. CONTRACT/GRANT NO
                                                           68-02-2093
                                                           Task Order  101
12 SPONSORING AGENCY NAME AND ADDRESS
 Environmental Sciences Research  Laboratory - RTP, NC
 Office of Research and Development
 U.S. Enviornmental Protection Agency
 Research Triangle Park, NC   27711	
                                                           13. TYPE OF REPORT AND PERIOD COVERED
                                                           Final
                                                          14. SPONSORING AGENCY CODE
                                                             EPA/600/09
15. SUPPLEMENTARY NOTES
16. ABSTRACT                                            .
     Ten of the 25 stations  making up the Regional Air Monitoring System were equipped
with dichotomous samplers  and high volume filter samplers  for aerosol measurements.
The high volume samplers collected samples every third day for 24-hour periods  (0000-
2400)..  Sample filters  were  returned to a chemical laboratory where weights of  total
suspended particulate  (TSP)  were determined, and wet chemical analyses performed  for
sulfates and nitrates.  A  total  of 2358 samples were obtained between March  1975 and
March  1977.  The report describes both the operation of the sampling network,  in-
cluding equipment maintenance, and analysis and quality  control procedures and  results.
     Analyses were made to determine seasonal and  spatial  variations of the three para-
meters measured.  The  station geometric mean concentrations of TSP varied from  33.0  to3
90.9 yg m"3, sulfate ranged  from 7.0 to 12.7 yg m"J, ajki nitrate from 2.3 to 3.8  pg  m
Sulfate showed the greatest  seasonal variation, peaking  in the summer months, and
nitrate the least, with no consistent patterns discernable.
     An Appendix  lists  all  individual sampling results  obtained.
stored in the RAPS  Data Bank in Research Triangle  Park,  N.C.
                                                                    These data  are
17
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
 *ATr pollution
 *Aerosols
 *Weight(mass)
 *Sulfates
 *Inorganic  nitrates
 *Seasonal variations
 *Spati»l distribution
                                              b.lDENTIFIERS/OPEN ENDED
                                                                           COS ATI I leld/t.roup
                                                                              13B
                                                                              07D
                                                                              07B
                                                                              04B
13 DISTRIBUTION STATEMENT
   RELEASE TO PUBLIC
                                              19 SECURITY CLASS (This Report)
                                               UNCLASSIFIED	
                                                                         21 NO OF PAGES
                                                                              112
                                              20 SECURITY CLASS (Thispage)
                                               UNCLASSIFIED
                                                                         22 PRICE
EPA Foitn 2220-1 (9-73)

-------
                                  TECHNICAL REPORT DATA
                           (I'lcasc rratl ImU-i/i Hum on the rci aw before completing)
  REPORT NO
 EPA-600/7-78-041
         PB-280-198
4 TITLE AND SUBT.TLE  POLLUTANT MEASUREMENTS IN PLUMES FROM
  POWER PLANTS AND  CITIES
  Summer 1975, February 1976, and February 1977
  A Project MISTT Report	
                                                          3 RECIPIENT'S ACCESSION-NO.
                                  5 REPORT DATE
                                    March 1978
                                  6 PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
                                                          8 PERFORMING ORGANIZATION REPORT NO.
  J. A. Ogren,  D.  L.  Blumenthal, J. A. Anderson
  and W. H. White
                                    MRI  77  FR-1511
9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Meteorology  Research,  Inc.
  464 West Woodbury  Road
  Altadena, California 91001
                                  10. PROGRAM ELEMENT NO.

                                    INE625 EA-07 (FY-77)
                                  11 CONTRACT/GRANT NO.
                                    68-02-2245
12 SPONSORING AGENCY NAME AND ADDRESS
  Environmental  Sciences Research Laboratory  -  RTP,  NC
  Office of Research and Development
  U.S. Environmental Protection Agency
  Research Triangle  Park, NC  27711	
                                   13. TYPE OF REPORT AND PERIOD COVERED

                                    Final 6/18/75-10/18/77	
                                  14 SPONSORING AGENCY CODE
                                    EPA/600/09
15. SUPPLEMENTARY NOTES
16 ABSTRAQT
       Airborne measurements of aerosols and polluted gases  in  urban and oower plant
  plumes were  conducted during the summer of 1975, February  1976,  and  February  1977
  in the vicinity  of St.  Louis, Missouri; Moss Landing, California; and Clearwater,
  Florida, respectively.   The principal objective was to characterize  the  physical
  and chemical behavior of these plumes under a variety of meteorological  conditions,
  with emphasis on sulfur transport and transformation.  Results illustrate  the
  regional nature  of air pollution.  The transport of well-defined urban plumes
  over 150 km  downwind of a city was documented during day and  night conditions.
  Power plant  plumes were sampled over 100 km downwind of the source at night and
  during the day over the ocean; strong dilution mechanisms  limited the sampling
  of power plant plumes to 40 km during the day over land.   Measurements indicated
  that, when the plume was not well mixed to the ground, the mass  flux of  sulfur  in
  the plume did not change with distance.  In urban plumes,  a significant  reduction
  in sulfur was found; only about one-third of the emissions were  transported beyond
  100 km downwind  of the city.

       New techniques used in this study included an airborne impactors system  for
  aerosol collection and atmospheric electrical measurements for plume tracting.
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
 * Air pollution
 * Aerosols
 * Sulfates
 * Sulfur dioxide
 * Sulfuric acid
   Electric power  plants
 * Plumes
Conversion
Measurement
Airplanes
                                             b.lDENTIFIERS/OPEN ENDED TERMS
Project MISTT
                                                c  COSATl I icld/droup
13B
07D
07B
10B
21B
13 DISTRIBUTION STATEMENT


  RELEASE TO  PUBLIC
                      19 SECURITY CLASS (ThisReport)

                       UNCLASSIFIED	
                                                                        21 NO OF PAGES
                      2O SECURITY CLASS (This page I

                        UNCLASSIFIED
                                                22. PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPC'-!T DATA
                            (I'll asc rrail InHiiit iiinia on tin- n i *<• hcjorc cnni/ili
 1. REPORT NO
    EPA-600/7-78-053
                      	L PB-279-999
4. TITLE AND SUBTITLE
   NITROGEN  DIOXIDE PHOTOLYTIC, RADIOMETRIC,AND
   METEROLOGICAL FIELD DATA
                                                            6 PERFORMING ORGANIZATION CODE
                                                           3 RECIPIbNT'S ACCESSION NO.
                                                            5 REPORT DATE
                                                             March 1978
 7 AUTHOR(S)
   J.E. Sickles, II,  L.A.  Ripperton, W.C. Eaton,  and
   R.S. Wright
                                                           8 PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
   Research Triangle  Institute
   Research Triangle  Park,  North Carolina
                                                           10 PROGRAM ELEMENT NO
                                                              INE625 EA-03 (FY-77)
                                            27709
                                                           11 CONTRACT/GRANT NO

                                                              Contract No. 68-02-2258
 12 SPONSORING AGENCY NAME AND ADDRESS
   Environmental Sciences Research Laboratory  - RTF, NC
   Office of Research and Development
   U.S. Environmental Protection Agency
   Research Triangle Park, North Carolina   27711
                                                           13. TYPE OF REPORT AND PERIOD COVERED
                                                              Final
                                                           14. SPONSORING AGENCY CODE
                                                              EPA/600/09
 15 SUPPLEMENTARY NOTES
 16. ABSTRACT                                                                       ~~~~~	~~

        Photolysis  of nitrogen dioxide  is  a  major reaction  resulting in the formation
   of ozone in the  troposphere.  The rate  constant, k^, for  the  photodissociation  of
   N02 is, under  ambient conditions, a  function of latitude,  solar zenith angle,  and
   cloud cover,- therefore, k^ is highly variable.
        Nitrogen  dioxide photolysis data for calculating k^,  and radiometric and
   selected meteorological data, all under a variety of meteorological conditions,
   were collected during the spring and fall, 1975.  Data from  this study can be  used
   to aid the modeling of tropospheric  photochemical air quality and smog chamber
   results.
17
                                KEY WORDS AND DOPUMENT ANALYSIS
                  DESCRIPTORS
   *Air pollution
   *Nitrogen dioxide
   •Photolysis
   *Reaction kinetics
   *Radiometry
   *Meteorological  data
                            Field tests
                                              I) IDENTIFIERS/OPEN ENDED TERMS
                                                                         C  COSATI I icId/Group
     13B
     07B
     07E
     07D
     14B
     04B
 9 DISTRIBUTION STATEMENT

    RELEASE TO  PUBLIC
                                              19 SECURITY CLASS (Tins Report)
                                                UNCLASSIFIED
21 NO OF PAGES

 192
                                              20 SECURITY CLASS (Thispage)
                                                 UNCLASSIFIED
                                                                         22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing)
1 REPORT NO
  EPA-600/8-78-014a
         PB:286-248
                                                          3 RECIPIENT'S ACCESSION NO
4 TITLE ANOSUBTITLE
  USER'S MANUAL FOR KINETICS MODEL AND OZONE
  ISOPLETH  PLOTTING PACKAGE
                                                          5 REPORT DATE
                                                             July 1978
                                  6 PERFORMING ORGANIZATION CODE
7 AUTHOR(S)

  Gary  Z. Whitten and H. Hogo
                                  8 PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Systems  Applications, Incorporated
  950 Northgate Drive
  San Rafael,  California  94903
                                  10. PROGRAM ELEMENT NO.

                                    1AA6Q3   (AC-ISI  FY  77
                                  11 CONTRACT/GRANT NO

                                    68-02-2428
 12 SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences Research  Laboratory-RTP,  NC
  Office  of Research and Development
  U.S.  Environmental Protection Agency
  Research Triangle Park, North Carolina   27711
                                  13. TYPE OF REPORT AND PERIOD COVERED
                                     Interim
                                  14. SPONSORING AGENCY CODE
                                     EPA/600/09
 15 .SUPPLEMENTARY NOTES   .      .,,,,.    .      ,^    .   i   j   T^ •  •  •     ncc-    c
  Prepared  in cooperation with the Monitoring and  Data Analysis Division, Office of
  Air  Quality Planning and  Standards,  U.S.  Environmental  Protection Agency
 16. ABSTRACT
        The Kinetics Model and Ozone  Isopleth Plotting Package (OZIPP) is a
  computerized model that simulates  ozone formation in urban atmospheres.
  OZIPP calculates maximum one-hour  average ozone concentrations given a
  set  of input assumptions about  initial precursor concentrations, light
  intensity,  dilution, diurnal and spatial emission patterns, transported
  pollutant concentrations, and reactivity of the precursor mix.  The re-
  sults of multiple simulations are  used to produce an ozone isopleth
  diagram tailored to particular  cities.  Such a diagram relates maximum
  ozone concentrations to concentrations of non-methane hydrocarbons and
  oxides of nitrogen, and can be  used  in the Empirical Kinetic Modeling
  Approach (EKMA) to calculate emission  reductions necessary to achieve
  air  quality standards for photochemical oxidants.  This user's manual
  describes the technical basis,  necessary and optional input data, com-
  puter code and the use of OZIPP.
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lDENTIFIERS/OPEN ENDED TERMS
                                               c  COSATI Held/Group
   *  Air pollution
   *  Ozone
   *  Hydrocarbons
   *  Nitrogen oxides
     Meteorology
     Atmospheric circulation
   *  Mathematical models
*Chemical kinetics
* Nomographs
^Programming Manuals
13B
07B
07C
04 B
12A
07D
20K
20A
05B
18. DISTRIBUTION STATEMENT
   RELEASE TO PUBLIC
                                              19 SECURITY CLASS (This Report)
                                              UNCLASSIFIED
                                               21 NO OF PAGES
                                                   251
                                                                        22 PRICE
EPA Form 2220-1 (9-73)

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the n verse before completing)
 1 REPORT NO
  EPA-600/8-78-014b
PB-287-768
                                                           3 RECIPIENT'S ACCESSION>NO.
4. TITLE AND SUBTITLE

  KINETICS MODEL  AND OZONE ISOPLETH PLOTTING PACKAGE
  COMPUTER PROGRAM
                           5 REPORT DATE
                              July  1978
                           6. PERFORMING ORGANIZATION CODE
7 AUTHOR(S)
  Gary Z. Whitten and H. Hogo
                                                           8. PERFORMING ORGANIZATION REPORT NO.
9 PERFORMING ORGANIZATION NAME AND ADDRESS
  Systems Applications, Incorporated
  950 Northgate Drive
  San Rafael,  California  94903
                            10. PROGRAM ELEMENT NO.

                              1AA603  (AC-18)  FY  77
                            11. CONTRACT/GRANT NO.
                                                             68-02-2428
 12. SPONSORING AGENCY NAME AND ADDRESS
  Environmental Sciences Research Laboratory-RTP, NC
  Office of  Research and Development
  U.S. Environmental Protection Agency
  Research Triangle Park, North Carolina   27711
                            13. TYPE OF REPORT AND PERIOD COVERED
                              Magnetic  Tape	
                           14. SPONSORING AGENCY CODE
                              EPA/600/09
15. SUPPLEMENTARY NOTES
  Prepared  in cooperation with the Monitoring and Data Analysis Division,  Office of
  Air Quality Planning and Standards, U.S.  Environmental Protection Agency
16. ABSTRACT
       The  Kinetics Model and Ozone Isopleth Plotting Package  (OZIPP)  is a computer
  program  (on magnetic tape) that simulates  ozone formation in urban  atmospheres.
  OZIPP calculates maximum one-hour average  ozone concentrations given a set of
  input assumptions about initial precursor  concentrations, light intensity, dilution,
  diurnal and spatial emission patterns,  transported pollutant concentrations, and
  reactivity of  the precursor mix.  The  results of multiple simulations are used to
  produce an ozone isopleth diagram tailored to particular cities.  Such a diagram
  relates maximum ozone concentrations to concentrations of non-methane hydrocarbons
  and oxides of  nitrogen, and can be used in the Empirical Kinetic Modeling Approach
  (EKMA) to calculate emission reductions necessary to achieve air quality standards
  for photochemical oxidants.
17.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
              b.lDENTIFIERS/OPEN ENDED TERMS
C.  COSATI I Idd/Group
  Computer  programs
                                             09B
18. DISTRIBUTION STATEMENT
  RELEASE  TO  PUBLIC
              19 SECURITY CLASS (This Report)
              UNCLASSIFIED
                                         21. NO. OF PAGES
                                              20 SECURITY CLASS (Thispage)
                                              UNCLASSIFIED
                                                                         22 PRICE
EPA Form 2220-1 (9-73)

-------
                                 •  TECHNICAL 'JEPORT DATA
                            (Hcasf read Instructions on ihc rt verse hcjorc completing)
1  REPORT NO

EPA-6QQ/9-78-Q2Qa
              PB-287-436
4 TITLE AND SUBTITLE
WORKSHOP  PROCEEDINGS ON PRIMARY SULFATE  EMISSIONS  FROM
COMBUSTION SOURCES
Volume  1.   Measurement Technology	
                                                           3 RECIPIENT'S ACCESSION NO.
                                       5 REPORT DATE

                                        August 197&
 4
R?
                                       6 PERFORMING ORGANIZATION CODE
7. AUTHORISE
                                                           8. PERFORMING ORGANIZATION REPORT NO
9 PERFORMING ORGANIZATION NAME AND ADDRESS
Kappa Systems,  Inc.
1501 Wilson  Boulevard
Arlington, Virginia
                                       10 PROGRAM ELEMENT NO

                                          1AD712   BC-52   (FY-78)
                                       11 CONTRACT/GRANT NO
                                                                 68-02-2435
12. SPONSORING AGENCY NAME AND ADDRESS
Environmental  Sciences Research Laboratory  -  RTP,  NC
Office of  Research  and Development
U.S. Environmental  Protection Agency
Research Triangle Park, N.C. 27711	
                                       13 TYPE OF REPORT AND PERIOD COVERED

                                          Final	
                                       14 SPONSORING AGENCY CODE
                                          EPA/600/09
15 SUPPLEMENTARY NOTES
16 ABSTRACT
Technical  papers  on techniques for measuring  primary sulfate emissions from combustion
sources,  presented at a workshop sponsored  by the U.S.  Environmental Protection Agency,
are compiled in Volume 1 of a proceedings.

The objectives  of the workshop were to  review and discuss current measurement methods
and problem areas for sulfur oxides emission  with attention focused on sulfuric acid,
sulfates,  and sulfur-bearing particulate matter;  to review and discuss emission data
from various combustion sources operating under different conditions which include
various pollutant controls, fuel composition, excess boiler oxygen, etc.; and to
delineate  and recommend areas in need of research and development effort.

Scientists were invited to present the  result of  their  studies on primary sulfate
emissions.   The 3-day workshop devoted  one  day to measurement technology, a second to
characterization, and a third to critical assessment of the presented papers and
development of  summary working group reports  on each half-day session of the initial
2 days.   Thirty-one papers were presented by  29 participants on measurements and
characterization.
last day.
Four working group  reports  were developed and summarized in the
17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                                     c  COSATI I ic)d/Croup
 * Air pollution
 * Sulfates
 * Emission
 * Combustion  products
 * Measurement
 * Collecting  Methods
                                                        13B
                                                        07B
                                                        21B
                                                        14B
18 DISTRIBUTION STATEMENT
                                              19 SECURITY CLASS (Tins Report}

                                                   UNCLASSIFIED	
                                                     21 NO OF PAGES

                                                         289
           RELEASE  TO PUBLIC
                          20 SECURITY CLASS /Tins page)

                               UNCLASSIFIED
                                                                         22 PRICE
 EPA Form 2220-1 (Rev. 4-77)    PREVIOUS E.DI TION is OBSOLET E

-------
                                  TECHNICAL REPORT DATA
                           (Please read Instructions on the reverse before completing)
 REPORT NO.
 EPA-600/J-78-057
                                                          3 RECIPIENT'S ACCESSION-NO
JOURNAL ARTICLE
 TITLE AND SUBTITLE

   OZONE TRANSPORT  IN  THE ST.  LOUIS AREA
                                                          5 REPORT DATE
                                                          erPERFORMING ORGANIZATION CODE
 AUTHOR(S)

   Thomas R. Karl
                         8. PERFORMING ORGANIZATION REPORT-NO.

                         .  1AA603  AD-08  (1977)
 PERFORMING ORGANIZATION NAME AND ADDRESS
                                                          10. PROGRAM ELEMENT NO.
                                                          11. CONTRACT/GRANT NO.
12 SPONSORING AGENCY NAME AND ADDRESS
 Environmental  Sciences Research Laboratory-RTP,  NC
 Office of Research  and Development
 U.S. Environmental  Protection Agency
 Research Trianole Park, NC  27711
                                                          13. TYPE OF REPORT AND PERIOD COVERED
                         14. SPONSORING AGENCY CODE
                              EPA/600/09
15. SUPPLEMENTARY NOTES
  REFERENCE: . Atmospheric Environment,  12(6-7):1421-1431,  1978
16. ABSTRACT
      Measurements from the Regional Air  Pollution Study in St. Louis,  and  from
  synoptic  rawinsonde stations in North America were used with annual  point  and
  area source emission data in St. Louis to  establish some consequences  of local
  and large-scale ozone transport.

      In rural  areas outside of St. Louis,ozone concentrations exceeded the National

  Ambient Air Quality Standard of 80 ppb (160 yg/m ) and could not be  attributed
  to the emissions of pollutants within the  metropolitan area of St. Louis.  Typically,
  these  high ozone concentrations occurred when the air flowing into St. Louis
  had been  associated with an anticyclone  during the 3 days prior to its arrival.
  Trajectories indicated that during these 3-day periods the air had remained
  within the eastern half of the United States where there are numerous  high-intensity
  urban-industrial centers.  On other days during the study analyses of  the local
  air flow  confirmed that the urban-industrial areas within the immediate vicinity
  of St. Louis were responsible for high ozone concentratipn in the city as well
  as in  the rural areas.  An analysis of the formation and'movement of an "ozone
  cloud" through the network of stations revealed the consequences of  local  ozone
  generation and transport.
17.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                             b.lDENTIFIERS/OPEN ENDED TERMS
                                         COS AT I Field/Group
  *Air pollution
  *0zone
  *Transport properties
                St.  Louis, MO
13B
07B
18. DISTRIBUTION STATEMENT

               RELEASE TO  PUBLIC
            19. SECURITY CLASS (This Report)
                  UNCLASSIFIED
                                                                        21. NO. OF PAGES
                                              20 SECURITY CLASS (This page)

                                                   UNCLASSIFIED
                                                                        22 PRICE
EPA Form 2220-1 (9-73)

-------
                                  • TECHNICAL REPORT DATA
                            (Please read Instructions on i v reverse before completing)
1. REPORT NO.

 EPA-600/9-78-020b
2.
     PB-287-437
4. TITLE AND SUBTITLE

 WORKSHOP  PROCEEDINGS ON PRIMARY SULFATE  EMISSIONS  FROM
 COMBUSTION  SOURCES
 Volume 2.   Characterization
                             3. RECIPIENT'S ACCESSION NO.
                             5 REPORT DATE

                                August 1978
                             6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S)
                                                           8. PERFORMING ORGANIZATION REPORT NO,
9 PERFORMING ORGANIZATION NAME AND ADDRESS
                                                            10 PROGRAM ELEMENT NO
 Kappa Systems,  Inc.
 1501 Wilson Boulevard
 Arlington, Virginia
                               1AD712   BC-52   (FY-78)
                              11 CONTRACT/GRANT NO.
                                                              68-02-2435
12. SPONSORING AGENCY NAME AND ADDRESS
 Environmental .Sciences  Research Laboratory  -  RTP,  NC
 Office of  Research  and  Development
 U.S. Environmental  Protection Agency.
 Research Triangle Park. N.C. 27711	
                             13. TYPE OF REPORT AND PERIOD COVERED

                                Final	
                             14. SPONSORING AGENCY CODE
                                EPA/600/09
15. SUPPLEMENTARY NOTES
16. ABST
        VCT
 Technical papers  on  the characterization of primary  sulfate emissions from combustion
 sources, presented at a workshop sponsored by  the  U.S.  Environmental  Protection Agency
 are compiled  in Volume 2 of a proceedings.

 The objectives of the workshop were to review  and  discuss  current measurement methods
 and problem areas for sulfur oxides emission with  attention focused on sulfuric acid,
 sulfates, and sulfur-bearing particulate matter; to  review and  discuss emission data
 from various combustion sources operating under different  conditions  which include
 various pollutant controls, fuel composition,  excess  boiler oxygen, etc.;  and to
 delineate and recommend areas in need of research  and development effort.

 Scientists were invited to present the result  of their  studies  on primary  sulfate
 emissions.  The 3-day workshop devoted one day to  measurement technology,  a second to
 characterization, and a third to critical assessment  of the presented papers and
 development of summary working group reports on each  half-day session of the initial
 2 days.  Thirty-one  papers were presented by 29 participants on measurements and
 characterization.  Four working group reports  were developed and summarized in the
 last day.
17.
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lOENTIFIERS/OPEN ENDED TERMS
                                                                        c.  COSATI Held/Group
 * Air pollution
 * Sulfates
 * Emission
** Combustion products
 * Chemical analysis
 * Physical properties
                                              13B
                                              07B
                                              21B
                                              07D
18 DISTRIBUTION STATEMENT
     RELEASE TO PUBLIC
                                              19 SECURITY CLASS (This Report)

                                                 UNCLASSIFIED
                                           21 NO OF PAGES

                                               287
                20 SECURITY CLASS (Tinspage)
22 PRICE
                                                 UNCLASSTFTFn
EPA Form 2220-1 (Rev. 4-77)   PREVIOUS EDITION is OBSOLETE

-------
                                   TECHNICAL REPORT DATA
                            (Please read Instructions on the reverse before completing)
 1 REPORT NO.
  EPA-600/J-78-058
                             2.
   JOURNAL ARTICLE
                                                           3 RECIPIENT'S ACCESSION NO.
4. TITLE AND SUBTITLE
                                                           5. REPORT DATE
  DAY OF THE WEEK VARIATIONS OF PHOTOCHEMICAL POLLUTANTS
  IN THE ST. LOUIS AREA
                                6«ft£RFORMING ORGANIZATION CODE
7. AUTHOR(S)
                                                           8. PERFORMING ORGANIZATION REPORT NO.
  Thomas R. Karl
9 PERFORMING ORGANIZATION NAME AND ADDRESS
                                                           10. PROGRAM ELEMENT NO.
                                                               1AA603  AD-05  (FY-77)
                                                           11. CONTRACT/GRANT NO.
 12 SPONSORING AGENCY NAME AND ADDRESS
 •Environmental Sciences  Research Laboratory - RTP, NC
  Office of Research and  Development
  U.S. Environmental Protection  Agency
  Research Triangle Park,  NC  27711
                                13. TYPE OF REPORT AND PERIOD COVERED
                                14. SPONSORING AGENCY CODE
                                    EPA/600/09
15. SUPPLEMENTARY NOTES
    REFERENCEr  Atmospheric  Environment, 12(8):1657-1678,  1978
16. ABSTRACT
 As part of the Environmental  Protection Agency's  Regional  A1r Pollution Study  (RAPS)*
 a network of 25 stations  continuously recorded aerometrlc  data 1n the Greater  St.  Louii
 area.  Various photochemical  pollutants (Ov NO,  N0«  and total hydrocarbons) and
 some selected meteorological  variables (wind speed/temperature, and solar radiation")
 were analyzed with respect to the day of the week using  11  months of data collected
 during the warm months of the year—periods during which Mgh ozone concentrations
 were common in St. Louis.   The results reveal that the sign (!) of the workday to
 Sunday differences in the concentration of ozone  depends to a large extent on  the
 distance of the measurement from the major emission area of the metropolitan area  of.
 St.  Louis.  The data suggest  that this 1s due to  the  Impact of nitric oxide on the •
 ambient ozone concentrations.   This appears to offer  at  least a partial explanation'
 for  some of the contrasting results reported by various  Investigators regarding the-
 differences 1n ozone concentrations between weekends  and weekdays.
 7.
                               KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTORS
                                              b.lDENTIFIERS/OPEN ENDED TERMS
                                             c.  COSATI Field/Group*
 * Air  pollution
 * Ozone
 * Nitrogen  oxide
 * Nitrogen  dioxide
 * Hydrocarbons
   Meteorological data
* Day
* Variations
St. Louis^MO
13B
07B
07C
04B
04A
18. DISTRIBUTION STATEMENT
           RELEASE TO PUBLIC
                                              19. SECURITY CLASS (This Report}

                                                   UNCLASSIFIED
                                                                         21. NO. OF PAGES
                   20 SECURITY CLASS (Tins page)
   JRITY CLASS (Tins p
   UNCLASSIFIED
                                             22. PRICE
EPA Form 2220-1 (9-73)

-------