&EPA
United States
Environmental Protection
Agency
Office of Research and Development
National Exposure Research Laboratory
Characterization Research Division
P. O. Box 93478
Las Vegas, NV 89193-3478
                                      June 1995
  National Exposure Research Laboratory
         Characterization Research
            Division-Las Vegas
       Superfund/RCRA Technology
              Support Project
   Technology Support Center
      for Monitoring and Site
      Characterization FY95
      Third Quarterly Report

           April-June 1995
4390odc95
               U.S. Environmental Protection Agency, Characterization Research Division - Las Vegas

-------
            UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

                    OFFICE OF RESGA.RCH AND DEVELOPMENT
                   NATIONAL EXPOSURE RESEARCH LABORATORY
                            P O BOX 93478
                       LAS VEGAS NEVADA 89193 3478
                                             Chataclen/aiion Research Division
                         August 17,  1995
MEMORANDUM;
SUBJECT:  National Exposure  Research Laboratory
          Characterization Research Division - Las Vegas
          Third Quarterly Report

FROM:     Kenneth W. Brown
          Director, Technpidiefy "StTpportT Center

TO:       Richard SteimleM5120W)
          Project Manager
          Superfund Technology Support Project

          David C. Bartenfelder  (5303W)
          RCRA Enforcement  Division
          Office of Work Program Enforcement

    . Attached is the  third quarterly report for  FY95  of  the
activities  of the Characrterization Research  Division -  Las
Vegas,  Technology Support Center (TSC).  This quarterly  report
includes  the months of April, May, and June 1995.  The total
superfund resources spent for those projects  identified  in the
attached  report was $179,809. The  resource distribution  included
$172,414, TSC, $4,500 PC&B,  and  Regional $2,895.  The  total RCRA
resources spent  for those projects identified in the  attached
report was  $18,480.

      The  following  Superfund projects  have  been  completed and
therefore deleted from this quarterly  report: Olean Wellfield SF
Site,  Solvent Savers  SF Site, Drake Chemical  SF  Site, Oak Ridge
SF Site,  Schuykill  Metals SF Site, Allied  Paper  SF Site, Apache
Powder SF Site,  Ogden SF Site,  Payson  SF  Site,  and Verdese Carter
Park SF Site.

      The following RCRA projects have  been completed  and
 therefore deleated from this quarterly report:   Southern
 California Chemical RCRA Facility, and TOSCO Refinery RCRA
 Facility.

-------
     If you need additional information, please call me at
(702)798-2270.

Attachment
cc:
Wayne N. Marchant, 0DC             Anders Denson, OPS/EXC125
Margaret Kelly, EPA Hdqtrs         Steve Hern, ASB/EXC210
John M. Moore, ODC                 Edward Kantor, OPS/EXC234
J. Gareth Pearson, ASB             Phillip A. Malley, LESAT
Christian G. Daughton, ASB/CHL     Bob Breckenridge,  INEL
Paul J. Weeden, RSB/ROC603         Alan Crockett, INEL
Richard Garnas, MSB/MSL6           Clare Gerlach, LESAT
Jane Denne, ASB/CAP

-------
                                     TABLE OF CONTENTS

                                      (Indexed by Site Name)
SUPERFUND	  1

    REGION 1 	  1
                                                Grace, W.R. SF Site	  1
                                                Loring AFB SF Site	  1
                                                O'Connor, F. SF Site	  2
                                                Pine Street Canal SF Site	  3
                                                Pownal Tannery SF Site	  4
                                                Western Sand & Gravel SF Site	  4
    REGION 2 	  5
                                                Diamond Alkali Site SF Site  	  5
                                                Lake Onondaga SF Site	  5
                                                Mercury Refining SF Site	  6
                                                Warwick Landfill SF Site	  6
    REGION 3 	  7
                                                Atlantic Wood Industries SF Site	  7
                                                Chem-Solv SF Site	  8
                                                Fort George Meade SF Site	  8
                                                Morgantown Ordnance SF Site	  9
                                                Naval Air Warfare SF Site	  9
                                                Naval Ships Control Center SF Site	   10
    REGION 4	   11
                                                Aberdeen Pesticide SF Site  	   11
    REGION 5 	   11
                                                Allied ChemicalAronton Coke SF Site	   11
                                                 Byron Salvage SF Site 	   12
                                                 Lorain County SF Site	   12
                                                 North Drive SF Site	   13
                                                 North Drive/Oak Street SF Site	   13
                                                 Petoskey Municipal SF Site	   14
    REGION 6	   14
                                                 RAB Valley SF Site	   14
                                                 South Cavalcade SF Site  	   15
    REGION 7  	   16
                                                 Kern-Pest Laboratories SF Site	   16
                                                 Lindsay Manufacturing SF Site	   16
    REGION 8	   17
                                                 Utah Power/Light-American Barrel SF Site  ....   17
    REGION 9	   17
                                                 Allied Signal SF Site  	   17
                                                 Carson River Mercury SF Site	   18
                                                 Concord Naval SF Site	   19
                                                 King Tut SF Site 	   20
                                                 Mare Island SF Site	   20
                                                 Mather AFB SF Site  	   21
                                                 McCormick-Baxter Wood-Treating SF Site	   21
                                                 Modesto SF Site  	   22
                                                 Montrose SF Site	   23
                                                 Phelps Dodge SF Site	   23
                                                 San Fernando SF Site 	   24

-------
   REGION 10  	   25
                                            ASARCO Smelter SF Site	   25
                                            Bunker Hill SF Site	   25
                                            Lyman Mining SF Site	   26

SUPERFUND SHORT-TERM REQUESTS	   27
                                            Short Term Requests	   27

RCRA CORRECTIVE ACTION	   29

   REGION 1  	   29
                                            Envirite RCRA Facility  	   29
   REGION 5  	   29
                                            Columbus Waste-To-Energy RCRA Facility	   29
                                            Metalworking Lubricants RCRA Facility 	   30
   REGION 8	   31
                                            EXXON Refinery RCRA Facility	   31
   REGION 9	   31
                                            GTE RCRA Facility 	   31
                                            Magna RCRA Facility	   32
                                            Quemetco RCRA Facility  	   33

RCRA SHORT TERM REQUEST	   34
                                            Short Term RCRA Technical Support	   34

SUPERFUND REMOTE SENSING SHORT TERM REQUEST	   35
                                            Superfund Short Term Remote Sensing Technical
                                                     Support 	   35

RCRA REMOTE SENSING SHORT TERM REQUEST	   36
                                            RCRA Short Term Remote Sensing Technical
                                                     Support	   36

ISSUE PAPER  	  37
                                            Identifying Background	  37
                                            Open Burn/Open Detonation	  38

COORDINATION 	  39
                                            Superfund Coordination	  39
                                            RCRA Coordination 	  39

TECHNOLOGY TRANSFER	  40
                                            Superfund Technology Transfer 	  40

-------
                                           SUPERFUND
REGION 1

•   Project Name:  W.R. Grace Superfund Site
    Site: Grace, W.R. SF Site
    Site ID:

    Type-Lead:
    Requested by: Lynn Jennings (617) 573-9634
    Lead Scientist: A.K. Singh (702) 435-3731

    Start Date: May 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: 55,000
    Revised Budget: S
    Major Contaminants: Organics
         Job Order No: 226 10106
Total Expenditures: S3,988
Total FY95 Expenditures: S3,988
Total 3rd Qtr. Expenditures: 53,988
    The Region I Remedial Project Manager (RPM) requested that the Characterization Research Division
    Las Vegas (CRD-LV), Technology Support Center (TSC) examine the use of a formula for an upper
    one-sided lOO(l-a) percent confidence limit, for assessing site sampling/monitoring data.  Three data sets
    were sent to the TSC for assessment.  The following statistical tests were performed on the data sets:

    •   Summary statistics and sample histograms of concentration data and log-transformed concentration
        data were computed using the software package GEO-EAS.

    •   Kolmogorov-Smirnov test was used to test normality and log-normality of the data using the
        software package SCOUT.

    •   Tests for outliers were performed on the data  using the software SCOUT.

    A report that provided the statistical assessment and recommendations titled, "Statistical Analysis of
    Battery Separation Lagoon Post Excavation Sampling Data for W.R. Grace Superfund Site" was provided
    to the RPM.
    Project Name: Loring AFB Superfund Site
    Site: Loring AFB SF Site
    Site ID:
          Job Order No: 224 10106
    Type-Lead:
    Requested by: Dick Willey (617) 573-9639
    Lead Scientist: Dr. Karl Pohlmann (702) 895-0485

    Start Date: January 1995
    Expected Completion Date: September  1995
    Revised  Completion Date:

-------
          UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

                   OFFICE OF RESEARCH AND DEVELOPMENT
                 NATIONAL EXPOSURE RESEARCH LABORATORY
                          P.O BOX 93478
                     LAS VEGAS. NEVADA 89193 3478
                                            CHARACTERIZATION RESEARCH DIVISION
                        September  15,  1995


SUBJECT:  Support Activities addressed by the Characterization
          Research Division, Las Vegas (CRD-LV) Technical Support
          Center
FROM:     Kenneth W. Brown
          Director, Technology Support Center
TO:      -JSJriu Hoang	—;=>
          Regional Scientist     /'

     Kim, please  find  attached the Third  FY95 Quarterly  Report  by
the CRD-LV TSC.   I have  been  requested  to provide  the  Regional
Scientist's with  information  pertaining to the  Regional  Technical
Support efforts addressed  by  the CRD-LV TSC.  I hope the
information in this  quarterly report  will be helpful to  your
program(s).  Also, I will  continue to send the  quarterly reports
to you for your information and  use.

     As you are aware,  each TSC  Director/Manager is required  to
provide the OSWER Program  Office, on  a  quarterly basis,
documentation of  resources spent per  site, activities/products,
expenses incurred, expected completion  dates, and budget
requirements.  The CRD-LV  TSC also keeps  the necessary budget
information for Regional cost recovery  actions.

     If I can be  of  further assistance  and/or if you need
additional information or  clarification pertaining to  the
attached report,  please call  me  at  (702)798-2270.

Attachment(s)

cc:w/o attachment:   Richard Steimle
                     J.  Gareth Pearson

-------
Estimated Budget: $5,000                                 Total Expenditures: PC&B $300
Revised Budget: S                                        Total FY95 Expenditures: PC&B $300
Major Contaminants: Organics                            Total 3rd Qtr. Expenditures: PC&B $300


The groundwater at Loring Air Force Base is currently being sampled to determine if contaminants have
migrated from soil sources. A Regional Groundwater Forum member requested that the CRD-LV TSC
review the sampling methods, statistical tests being utilized, and determine if the design (numbers of
samples) is adequate.  Specific questions that needed to be addressed by the CRD-LV TSC were:

•  Is there sufficient data to draw meaningful conclusions?

•  Is the quality of the data adequate?

•  Was  the data analyzed in an appropriate manner?

•  Are the conclusions made by the Air Force supported by the data?

The TSC reviewed the document titled, "Field Data Validation Study Report  for Debris  Disposal Areas
Operable Unit(OU3)  Loring AFB, Maine", dated October,  1994. The TSC provided a letter report with
the following summary conclusions:

The report is flawed due to the inadequate presentation of the data, the inconsistencies in the data and their
interpretation, the apparent lack of adequate interpretation of all the available data, and the misuse of
statistical analytical methods.  These flaws may act to conceal differences between the methods or may
emphasize differences that do not physically exist.  In any case, the uncertainty in the results causes the
conclusions to be questionable. Additional reviews of site documents  may be required.
 Project Name: F. O'Connor Company
 Site: O'Connor, F. SF Site
 Site ID:                                                 Job Order No: 224 01109

 Type-Lead:
 Requested by: Ross Gilleland (617) 573-9662
 Lead Scientist: A.K. Singh (702) 435-3731

 Start Date: February  1995
 Expected Completion Date: September 1995
 Revised Completion Date:

 Estimated Budget: $10,000                                Total Expenditures: $ 5,460
 Revised Budget: $                                        Total FY95 Expenditures: $ 5,460
 Major Contaminants: PCBs                               Total 3rd Qtr. Expenditures: S 2,778

 A geostatistical analysis of the distribution of soil contaminated with polychlorinated biphenyls (PCBs)
 was conducted to develop the sampling plan for the F. O'Connor Superfund Site in Augusta, Maine.
 The analysis was designed to support attainment of target cleanup goals as specified in the U.S.
 Environmental Protection Agency (EPA) Record of Decision (ROD) for the Site. Over 450 soil samples
 were collected during Remedial Investigation and pre-design phases of the study. Chemical analyses on
 these samples were performed for PCBs using both laboratory and field  screening methods.  Samples

-------
   were initially collected at grid locations, while subsequent samples were collected to define areas of
   higher concentrations and to determine the clean boundaries of the site.

   Analysis of the comprehensive data set as well as data subsets indicated a log-normal distribution of the
   data.  Data subsets were developed based on knowledge of waste disposal and contaminant distributions.
   Variogram analysis was conducted using indicator parameters corresponding to the ROD specified
   threshold limits of 1 and 10 ppm PCBs.

   The RPM has requested that the CRD-LV TSC evaluate the geostatistical model used by the PRP, the
   use of the geometric mean to establish compliance with the cleanup criteria, and to comment on the use
   of composite samples. CRD-LV personnel reviewed the provided data  and submitted an initial response.
   Additional reviews of the  utilized statistical procedures are in process.

•  Project Name:  Pine Street Canal
   Site:  Pine Street Canal SF Site
   Site ID: 01NHG1                                       Job Order No: 224 101%

   Type-Lead:
   Requested by:  Ross Gilleland (617) 573-5766
   Lead Scientist: M. Silverstein (702) 897-3291/D. Jackson (702)

   Start Date: July 1994
   Expected Completion Date: March 1995
   Revised Completion Date: September 1995

    Estimated Budget: S25.000                       Total  Expenditures: 558,669, PC&B S1600
    Revised Budget: $40,000                         Total  FY95 Expenditures: $42,245, PC&B $1100
    Major Contaminants:  PAH                      Total  3rd Qtr. Expenditures: $3,707, PC&B $400

   The Region  1  Project Officer requested that approaches be examined to determine whether the Pine
    Street Canal site characterization techniques are addressed  sufficiently: A sampling/monitoring approach
    for confirming the vertical and lateral extent of soil/sediment contamination, procedures for identifying
    levels of soil, sediment, and possibly water contamination, the quality assurance/quality control (QA/QC)
    plan, the S&A plan and all other methods being proposed to fully  characterize the site  for remedial
    purposes. In addition, an assessment of data needs necessary to satisfy the characterization objectives
    was required.  This data assessment involved data interpretation and recommendations involving
    statistical and  other tests necessary for making decisions concerning the extent of site contaminants.

    To characterize site contaminants, the selection of an appropriate immunoassay kit was an important
    factor in successfully completing the site characterization objectives. Addressing this effort required
    CRD-LV scientist(s) to identify critical elements that must be implemented by the PRPs to validate the
    immunoassay technology.  In addition, TSC scientist(s) will be required to assess the validation
    process/procedures and the data obtained.

    Following the  review and acceptance of the Work Plan, providing on-site oversight and field audit for the
    "Preliminary Soil/Sediment Screening/Sampling" of  the Phase I ARI activities conducted by the PRPs was
    required.  Field audit oversight included observing and documenting the field activities, and analyzing
    split samples using fix-lab analysis. During this quarter numerous reviews of site documents were
    completed.  Split samples were collected and sent to CRD-LV for  analysis.  The analysis was completed
    during this quarter. In addition, a field on-site audit was  completed. The results of the audit with
    suggestions and recommendations were sent to the RPM. The initial draft of the data validation report
    was provided to the RPM.

-------
•   Project Name:  Pownal Tannery Sample Analysis
    Site: Pownal Tannery SF Site
    Site ID:                                                Job Order No: 226 10106

    Type-Lead:
    Requested by: Terrance Connelly (617) 573-9638
    Lead Scientist: Neal Amick (702) 897-3231

    Start Date:  May 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: $15,000                      Total Expenditures: $142
    Revised Budget: S                              Total FY95 Expenditures: S142
    Major Contaminants: Dioxins/Furans             Total 3rd Qtr. Expenditures: $142

    The Pownel Tannery Site is a pre-NPL Site that has been approved for inclusion in the SACM process.
    A removal action in 1993 documented the presence of metals, volatile and semi-volatile organics, and
    dioxins/furans. Developing a statistical evaluation of the risk posed by site contaminants required the
    analysis of a large number of samples. Obtaining the required data base required a cost and time
    effective analytical procedure. The RPM has requested the use of the Field-Portable Scanning
    Spectrofluorometer  (FPSS) to measure dioxins/furans levels in site samples.  To determine if the FPSS is
    a suitable measurement method, the RPM has sent site samples to the TSC for FPSS analysis. The
    analyses of these samples was initiated this quarter.
 •   Project Name:  Western Sand & Gravel Data Review
    Site: Western Sand & Gravel SF Site
    Site ID:                                                 Job Order No: 226 10106

    Type-Lead:
    Requested by: Al Klinger (617) 573-9662
    Lead Scientist: A.K. Singh (702) 435-3731

    Start Date: June 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: S5,000                       Total Expenditures: Sl,424
    Revised Budget: S                             Total FY95 Expenditures: $1,424
    Major Contaminants:  Organics                  Total 3rd Qtr. Expenditures: $1,424

    A number of years ago, the CRD-LV TSC provided statistical support to the RPM pertaining to the
    Wilcoxen Test to compare theoretical verses observed data. This effort was in  support of completing the
    ROD. Relative to the Wilcoxen Test, the  RPM provided the TSC with some site data (benzene levels in
    groundwater) for assessing "Outliers".  The TSC provided the RPM with an assessment of the data that
    included:


     •  An assessment pertaining to the normal data distribution, and

                                                  4

-------
    •   Statistical tests for Outliers using the following two options: (a) classical, and (b) Huber's Robust
        Procedure.

    In addition to the statistical assessment, recommendations and conclusions pertaining to the data analysis
    were provided.
REGION 2
•   Project Name:  Diamond Alkali
    Site: Diamond Alkali Site SF Site
    Site ID:                                                Job Order No: 224 10179

    Type-Lead: Fund
    Requested by: Lance Richman  (214) 264-6695
    Lead Scientist: A.K. Singh (702) 435-3731, J.R. Donnelly

    Start Date: July 1993
    Expected Completion Date: February 1994
    Revised Completion Date: September 1995

    Estimated Budget: 530,000                               Total Expenditures: S27,507
    Revised Budget: S                                       Total FY95 Expenditures: $1,325
    Major Contaminants: Organics, PCBs                     Total 3rd Qtr. Expenditures: $713

    The RPM requested that  the TSC provide a quality assurance and RI review.  In addition, a review of
    the suggested monitoring design approach was requested.  CRD-LV provided a report that addressed QA
    aspects and provided a number of suggestions that would enhance the identity of the geographical
    distribution of PCBs in sediments  in the Passaic River.  CRD-LV has assisted the RPM in negotiations
    with the PRPs and assisted in the  development of a definitive monitoring design approach. CRD-LV
    scientists received the final S&A Plan developed by the PRPs.  Comments and suggestions  pertaining to
    the final S&A Plan were provided to the RPM. Recommendations and comments pertaining to suggested
    statistical tests were provided to the RPM. A request to assess available  dioxin analytical methods was
    received. Recommended analytical procedures were provided to the Region.


 •  Project Name: Lake Onondaga Sample Analysis
    Site: Lake Onondaga SF Site
    Site ID:NYD 986913580                                 Job Order No: 226 10106

    Type-Lead:
    Requested by: Herb King (212) 637-4268
    Lead Scientist: Dave Dobb (702) 897-3273

    Start Date: June 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

-------
   Estimated Budget: S 15,000                      Total Expenditures: S783
   Revised Budget: S                             Total FY95 Expenditures: S783
   Major Contaminants: Mercury                  Total 3rd Qtr. Expenditures: S783

   This site is relatively small (4.5 square miles) that has been contaminated by discharging waste streams
   containing mercury and other heavy metals.  The RPM was interested in having the CRD-LV TSC
   analyze a number of sediment and water samples for the presence of mercury.  The analysis of these
   samples would include the determination of organic, water soluble, acid soluble, metallic and mercury
   sulfide fractions.

   The CRD-LV TSC has not received any samples from the site at this point in time. A final decision
   concerning the analysis will be made by the RPM and State of New York personnel.


   Project Name:  Mercury Refining Data Sample Analysis
   Site: Mercury Refining SF Site
   Site ID:                                                 Job Order No: 226 10112

   Type-Lead:
   Requested by: Thomas Taccone (212) 264-9128
   Lead Scientist: Dave Dobb  (702) 897-3273

   Start Date: June 1995
   Expected Completion Date: September 1995
   Revised Completion Date:

   Estimated Budget: $10,000                      Total Expenditures: $1,539
   Revised Budget: S                             Total FY95 Expenditures: 51,539
   Major Contaminants: Mercury                  Total 3rd Qtr. Expenditures: $1,539

   The Region II RPM requested that the CRD-LV TSC analyze about ten (10) soil samples collected from
   the Mercury Refining Site for individual mercury species. The determination of various mercury species
   in these samples will allow  the RPM and the State of New Jersey to determine the risk posed by
   bioavailable species. The following mercury species will  be analyzed: organic (e.g. CH3HgCl); water
   soluble (e.g. HgQ); and soluble (i.e. HgO and HgSO4); metallic (HgO and amalgams); and mercury
   sulfide (HgS).

   The samples were received and are currently being analyzed.  A final report identifying the results will be
   provided to the RPM during the fourth quarter FY95.
•   Project Name:  Warwick Landfill
    Site: Warwick Landfill SF Site
    Site ID: NYD980506679                                 Job Order No: 226-10106

    Type-Lead: Remedial
    Requested by:  Damion Duda (212) 264-9589
    Lead Scientist: Steve Pyle  (702) 798-2529

-------
   Start Date: January 1994
   Expected Completion Date: September 1993
   Revised Completion Date: September 1995

   Estimated Budget: S 10,000
   Revised Budget: S
   Major Contaminants: Organics
Total Expenditures: S 6,149, PC&B 55,800
Total FY95 Expenditures: S 6,149, PC&B $2,900
Total 3rd Qtr. Expenditures: S 0, PC&B $1,200
   The RPM requested that CRD-LV provide technical assistance in finding an analytical method to analyze
   cellosolves in environmental samples. The CRD-LV ASB tested the feasibility of using a quick-turn-
   around method using direct aqueous injection (DAI) by analyzing five test compounds.  The results of
   these tests were provided to the RPM. The TSC has requested  from the RPM samples from the site be
   sent to CRD-LV to definitively test the DAI method. The Region sent samples to CRD-LV for analysis.
   The samples were analyzed, and a report titled, "Report on Warwick Sample Analysis Using Direct
   Aqueous Injection GC/MS Methodology" was sent to the RPM. The RPM requested additional
   explanation of the reported results.  Explanations were provided to the Region.
REGION 3
    Project Name:   Atlantic Wood Industries (AWI) Superfund Site
    Site: Atlantic Wood Industries SF Site
    Site ID:                                                Job Order No: 22601110

    Type-Lead:
    Requested by: David J.  lacono (215) 597-8485
    Lead Scientist: Neal Amick (702) 897-3231

    Start Date: May 1995
    Expected Completion Date: September 1995
    Revised Completion Date:
    Estimated Budget: S20,000
    Revised Budget: S
    Major Contaminants: Organics
 Total Expenditures: 57,570
 Total FY95 Expenditures: S7,570
 Total 3rd Qtr. Expenditures: S7,570
    The Atlantic Wood Industries (AWI) PRP's are planning to conduct an EPA-approved removal action
    that requires the excavation of about 520 cubic yards of contaminated sediments.  PAH's are the primary
    contaminants in the sediment(s). The RPM was required to make decisions pertaining to the boundaries
    (width and depth) of the excavation as a function of the cleanup standards.

    The RPM requested that the CRD-LV TSC assist in making on-site measurements of PAHs using the
    Field-Portable Scanning Spectrofluorometer (FPSS) during the removal phase.  In support of this request
    on-site FPSS measurements were made. The data obtained  from the FPSS was used to identify levels
    and the distribution of PAHs during the removal.  A report identifying the measurements will be
    provided to the RPM.

-------
Project Name: Chem-Solv Superfund Site
Site: Chem-Solv SF Site
Site ID:

Type-Lead:
Requested by: Debra Rossi (215) 597-9238
Lead Scientist: A.K. Singh (702) 435-3731

Start Date: June 1995
Expected Completion Date: September 1995
Revised Completion  Date:

Estimated Budget: S6,000
Revised Budget: $
Major Contaminants: Organics
         Job Order No: 226 10106
Total Expenditures: S3,632
Total FY95 Expenditures: 53,632
Total 3rd Qtr. Expenditures: S3,632
The PRP's developed and have proposed to use a statistical procedure for assessing and identifying
trends in groundwater contaminants at this site.  Based on the trends analysis, the PRP's will identify the
time period required to attain and meet the specified cleanup standards.

The RPM requested that the CRD-LV TSC review the proposed procedure and determine if this method
would be acceptable in satisfying the sites cleanup objectives. The TSC assessed the suggested approach
and provided the RPM with comments and suggestions in a report titled, "Some Recommendations for
Statistical Analysis of VOC Concentrations in Groundwater from the Chem-Solv, Inc. Superfund Site."
Project Name: Fort George Meade
Site: Fort George Meade SF Site
Site ID:

Type-Lead:
Requested by: Drew Lausch (215) 597-3161
Lead Scientist: A.K. Singh (702) 435-3731
          Job Order No: 224 10106
Start Date: January 1994
Expected Completion Date: April 1995
Revised Completion Date: September 1995

Estimated Budget: 56,000
Revised Budget: S
Major Contaminants: Inorganics/Organics
          Total Expenditures: $4,785, PC&B $400
          Total FY95 Expenditures: PC&B $400
          Total 3rd Qtr. Expenditures: PC&B $400
The objective of this Region III request is to determine the extent of which two completed UXO surveys
have attained a more stringent detection/removal requirement specified in the DOD-DOI transfer
agreement. In order to ascertain the effectiveness of the previous UXO surveys, DOD outlined the
following technical approach: (1) develop a UXO sampling plan; (2)  conduct a UXO survey; (3)
perform a statistical analysis on data obtained from the UXO survey and (4) evaluate potential impacts
to human health from UXO by employing a probabilistic risk assessment.  The TSC provided an initial
assessment of the past surveys. Based on the TSC comments and recommendations, a meeting with the
RPM, DOD, and CRD-LV scientist(s) was  held at CRD-LV. The TSC is involved with the statistical

-------
design approach and data assessment. Additional design approach reviews and geostatistical data
assessments are anticipated.


Project Name:  Morgantown Ordnance Works NPL Superfund Site
Site: Morgantown Ordnance SF Site
Site ID:                                                 Job Order No: 226 10106

Type-Lead:
Requested by: Melissa Whittington (215) 597-1286
Lead Scientist: A.K. Singh (702) 435-3731

Start Date: April 1995
Expected  Completion Date: September 1995
Revised Completion Date:

Estimated Budget: S7,000                       Total Expenditures: S4,130
Revised Budget: S                              Total FY95 Expenditures: S4.130
Major Contaminants:  Organics                  Total 3rd Qtr. Expenditures: $4,130

The Region III RPM  requested assistance in the proper use of statistical tests pertaining to a
biotreatability remedial study at the Morgantown site.  The following issues were identified by the RPM:

•  For a T-Test, when is the Paired T-Test used?
•  When is a 2-tailed test used?
•  When making the comparison using a T-Test, does n (number) have to be the same?, and
•  When is it appropriate to pool data sets?


The TSC provided  the RPM with the report titled, "Comments on Statistical Tests Pertaining to a
Biotreatability Remedial Study for Morgantown Ordnance Works NPL Superfund Site." The questions
asked by  the RPM  were addressed in the report.  In addition, statistical calculations using site data was
provided  along with suggested recommendations.

TSC personnel also participated in discussions with the PRP's pertaining to the use of suggested
statistical tests.


 Project Name:  Naval Air Warfare Center (NAWC)
 Site: Naval Air Warfare SF Site
 Site ID:                                                 Job Order No: 224 01102

 Type-Lead:
 Requested by: Darius Ostrauskas (215)  597-0549
 Lead Scientist:  D. Jackson/Glen Carpenter (208) 526-4166


 Start Date: November 1994
 Expected Completion Date: September 1995
 Revised  Completion  Date:

-------
Estimated Budget: S 10,000
Revised Budget: S
Major Contaminants: Organics
         Total Expenditures: 56,880
         Total FY95 Expenditures: S6,880
         Total 3rd Qtr. Expenditures: SO
The TSC was requested by the Region III RPM to examine suggested site characterization approaches to
determine if these approaches would be adequate to define the levels and geographical extent of site
contaminants. The initial effort of this review focused on the following two areas:  The first
was to review and comment on the results of the Phase I RI Soil Gas and Geophysical surveys. The
second was to review and comment on the additional Soil Gas and Geophysical survey work being
proposed in the Draft Phase III work plan. Additional efforts may focus on all suggested
sampling/monitoring contamination,  procedures for identifying levels of soil, sediment, and possible water
contamination, the quality assurance/quality control  (QA/QC) plan, the S&A  plan and all other methods
that are being proposed to fully characterize the site for remedial purposes.  In addition, an assessment
of data needs necessary to satisfy  the characterization objectives may be required if past characterization
efforts have not adequately characterized the sites contaminants.  This  data assessment could involve data
interpretation and recommendations involving statistical and other tests necessary for making decisions
concerning the extent of site contaminants.  The design of additional sampling/monitoring approaches
may be required.

The TSC completed a review of the  Phase I RI Soil-Gas and Geophysical Survey Report. Comments and
suggestions were provided to the  RPM. Additional data assessments and site  document reviews are
anticipated.
Project Name: Naval Ships Parts Control Center (SPCC) Superfund Site
Site: Naval Ships Control Center SF Site
Site ID:                                                 Job Order No: 226 10106

Type-Lead:
Requested by: Andrew Sochanski (215) 597-3167
Lead Scientist: A.K. Singh (702) 435-3731

Start Date: May 1995
Expected Completion Date: September 1995
Revised Completion Date:
 Estimated Budget: 58,000
 Revised Budget: S
 Major Contaminants: Dioxins
Total Expenditures: 54,202
Total FY95 Expenditures: 54,202
Total 3rd Qtr. Expenditures: 54,202
 The Region III RPM requested technical assistance in developing a monitoring design for sampling a
 biopile to determine the levels and distribution of dioxin contamination. The biopile consisting of about
 15,000 cubic yards of contaminated soil excavated from burn pits is six (6) feet deep, 240 feet in width
 and 390 feet long.

 The TSC provided the report titled, "Design for Dioxin Sampling - Navy Ships Parts Control Center,
 Burn Pits (Site 3), Mechanicsburg, PA". This report identifies the number of samples required to
 characterize the dioxin contamination and also provides various statistical tests that can be used to assess
 the resultant data.
                                               10

-------
REGION 4
    Project Name:  Aberdeen Pesticide Dumps NPL Superfund Site
    Site: Aberdeen Pesticide SF Site
    Site ID:                                                Job Order No: 226 10106

    Type-Lead:
    Requested by: Kay Crane (404) 347-7791 Extension: 2079
    Lead Scientist: A.K. Singh (702) 435-3731
    Start Date: June 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: $10,000                      Total Expenditures: SO
    Revised Budget: S                              Total FY95 Expenditures: $0
    Major Contaminants: Organics                  Total 3rd Qtr. Expenditures: $0

    The Region IV RPM requested that the CRD-LV TSC review a soil remedial design that was proposed
    by the PRP's.  The design and the statistical tests required to assess cleanup attainment were provided in
    a "Data Acquisition Report/Preliminary Cutline Document and a Design Criteria Report".

    The TSC reviewed  the documents and provided suggestions and recommendations for improving the
    suggested approach. The PRP's are currently reviewing the TSC recommendations.
REGION 5
    Project Name: Allied Chemical/Ironton Coke Superfund Site
    Site: Allied ChemicalAronton Coke SF Site
    Site ID:                                                Job Order No: 226 10106

    Type-Lead:
    Requested by: Thomas Alcamo (312) 886-7278
    Lead Scientist: Neal Amick (702) 897-3231

    Start Date: May  1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: $20,000                               Total Expenditures: $142
    Revised Budget:  $                                      Total FY95 Expenditures: $142
    Major Contaminants:  PAHs                             Total 3rd Qtr. Expenditures: $142

    The Allied Chemical site is a former coke plant that has five lagoons that were used for wastewater
    treatment and disposal.  The site remedy consists of incineration of approximately 122,000 cubic yards of
    lagoon five wastes along with other contaminated materials having  contaminant concentrations greater

                                                 11

-------
than 1000 ppm.  The primary contaminants are four carcinogenic PAHs (benzo (a) pyrene), chrysene,
benz (a) anthracene and dioenz (a,h) anthracene).

The remedial approach requires that the contaminated materials be screened and segregated prior to
incineration.  To address this screening requirement, the RPM has requested that the CRD-LV TSC
provide on-site PAH measurements using the Field Portable Scanning Spectrofluormeter (FPSS).

Because of the uncertainty pertaining to the FPSS's performance in adequately measuring these PAHs,
the RPM sent samples from the site to Las Vegas for analysis.  The TSC is currently in the process of
samples analysis.  Following the analysis, an assessment of the FPSS performance will be completed.


Project Name: Byron Salvage Yard
Site: Byron Salvage SF Site
Site ID:                                                 Job  Order No:

Type-Lead:
Requested by: Doug Yeskis (312) 886-0408
Lead Scientist: Alan Crockett (208) 526-0603/Bob Starr INEL

Start Date:  March  1995
Expected Completion Date: September 1995
Revised Completion Date:

Estimated Budget: $10,000                                Total Expenditures: 58,921
Revised Budget: S                                       Total FY95 Expenditures: $8,921
Major Contaminants:  VOCs                              Total 3rd Qtr.  Expenditures: $8,686

A Regional  Groundwater Forum member requested CRD-LV TSC's assistance in reviewing soil-gas work
completed on the Byron Salvage Yard Superfund site. The Byron Salvage Yard site is located in Byron,
Illinois in an area with fractured dolomite/limestone overlain by approximately 10 feet of glacial till.  The
till is mainly composed of sandy loam. The depth to groundwater is  approximately 65-70 feet below
ground surface.

The specific issues which require TSC's attention are related to whether soil-gas concentrations are
related to volatilization  for the groundwater, or indicative of a source of VOCs directly from a nearby
disposal area. An initial assessment of the data was completed and provided to the  Region.


Project Name: Lorain County  Pesticide Superfund Site
Site: Lorain County SF  Site
Site ID: 95-5T-05F-TFA-050B8                           Job Order No: 226 10106

Type-Lead:
Requested by: Steve Renninger (216) 835-5200/Mike Murphy (216) 323-9540 Site Location
Lead Scientist: Dave Atkinson (208)526-9745 INEL

Start Date: April 1995
Expected  Completion Date: November 1995
Revised Completion Date:
                                              12

-------
Estimated Budget: S 15,000                                Total Expenditures: $4,677
Revised Budget: $                                       Total FY95 Expenditures: $4,677
Major Contaminants: Methyl Parathion                    Total 3rd Qtr. Expenditures: 54,677

The Regional On-Scene Coordinator requested that CRD-LV assist in measuring levels of methyl
parathion that was sprayed in a number of homes in Lorain County, Ohio. This request will involve on-
site measurements using the innovative technology, "Ion Mobility Spectrometry."  Problems using this
measurement technology were identified prior to the on-site effort.  At this time, efforts to solve the
measurement problem(s) are being addressed.


Project Name:  North Drive Site
Site: North Drive SF Site
Site ID:                                                 Job Order No: 224 10187

Type-Lead:
Requested by: Tim Prendiville (312) 886-5122
Lead Scientist:  Ed Heithmar (702) 798-2626/D. Dobb (702) 897-3273

Start Date: November 1993
Expected Completion Date: July 1994
Revised Completion Date: September  1995

Estimated Budget: 540,000         Total  Expenditures: $68,584, TSC $54,770,Region 513,814,
                                 PC&B 53,200
Revised Budget: 570,000          Total FY95 Expenditures: TSC $0, Region $13,814, PC&B 5700
Major Contaminants:  Cyanide     Total 3rd Qtr. Expenditures: TSC SO, Region $, PC&B 5400

The RPM requested that the TSC evaluate available cyanide analytical methods to determine which
method should be used to quantify the amount of cyanide that  is bioavailable. Because of the widespread
contamination  in the area, the region also requested technical support to assist in the development of a
sampling plan.  The  TSC has been requested to provide input on sample numbers and the location of
sampling sites that will characterize site contaminants.  Site samples were collected and sent to  CRD-LV.
A QAPjP was written and sent to the  Region. The samples were analyzed. The analytical results were
provided to the Region in a document titled, "Determination of Total, Weak Acid Dissociable and
Bioavailable C anide in North Drive Samples". Additional samples from the site were collected and sent
to CRD-LV for analysis. Analysis of these samples was completed. A report of the analytical results was
provided to the Region. Additional explanation of the results was provided to the Region.


Project Name:  North Drive Site/Oak  Street  Superfund Site
Site: North  Drive/Oak Street SF Site
Site ID:                                       Job Order No:  224 10106

Type-Lead:
Requested by:  Rose Ellison (312) 692-7269
Lead Scientist: Laurie Ottmar (702) 897-3473

Start Date:  May 1995
Expected Completion Date: September 1995
Revised Completion Date:
                                              13

-------
  Estimated Budget: 515,000
  Revised Budget: S
  Major Contaminants: Cyanide
Total Expenditures: S 2,895, TSC SO, Region S2,895, PC&B $600
Total FY95 Expenditures: TSC SO, Region $2,895, PC&B 5600
Total 3rd Qtr. Expenditures: TSC SO, Region S2.895, PC&B $600
  The Regional OSC requested that the CRD-LV TSC evaluate available cyanide analytical methods to
  determine which method should be used to quantify the amount of cyanide that is bioavailable. Site
  samples were collected and sent to CRD-LV.  Prior to sample analysis, a QAPjP and SOP were
  approved.

  The samples were analyzed and the results provided to the Region in a document titled, "Determination
  of Total, Weak Acid Dissociable and Bioavailable Cyanide in North Drive/Oak Street Soil Samples."
  Because of the high leads of cyanide encountered, a number of modifications in the methods used were
  made. These modifications  included reduced sample sizes for distillation and the use of ion
  chromatography rather than pyridine-barbituric acid derivitization/colorimetry for determination of Total,
  WAD and bioavailable cyanides.
   Project Name: Petoskey Municipal Well Field
   Site: Petoskey Municipal SF Site
   Site ID: MID006013049
               Job Order No: 224 10197
   Type-Lead:
   Requested by: Terese Van Donsel (312) 353-6564
   Lead Scientist: Joe Donnelly (208) 897-3387/Wayne Sovocool (702) 798-2212

   Start Date: October 1994
   Expected Completion Date: December 1995
   Revised Completion Date:
   Estimated Budget: 525,000
   Revised Budget: S
   Major Contaminants: Organics
               Total Expenditures: Sl,554
               Total FY95 Expenditures: 51,554
               Total 3rd Qtr. Expenditures: $156
   The TSC was requested by the Regional RPM to provide analytical support. A number of site matrices
   are involved. For example, nearby wells contain volatile organic compounds such as trichloroethylene.
   In addition, because of the use and disposal of spent solvents and/or paint sludges, the soils are
   contaminated with high levels of VOCs and SVOCs and elevated levels of metals. A hydraulic fluid
   release also complicated the contaminant profile of both soils and groundwaters.

   Because of the large number of tentatively identified compounds  (TICs) in the site matrices, the CRD-
   LV will receive samples for analysis.  The TICs fingerprinting analysis is currently on hold.
REGION 6
    Project Name: RAB Valley Wood Preserving Superfund Site
    Site: RAB Valley SF Site
    Site ID:                                       Job Order No: 226 01107
                                                 14

-------
Type-Lead:
Requested by: Lon Biasco (214) 665-6673
Lead Scientist: Neal Amick (702) 897-3231

Start Date: December 1994
Expected Completion Date: June 1995
Revised Completion  Date: September 1995

Estimated Budget: 525,000
Revised Budget: S
Major Contaminants: PCP,  PAHs, Dioxins
Total Expenditures: S29,802
Total FY95 Expenditures: 529,802
Total 3rd Qtr. Expenditures: 512,655
The RAB Valley Wood Preserving Site covers approximately 30 acres in a predominately rural area
southeast of Panama, LeFlore County, Oklahoma.  The site was utilized as a wood preserving facility
from the early 1900s until 1976, when the wood treatment operations were abandoned.

Hazardous substances associated with wood preserving operations (i.e.,  PCP and the PAH components of
creosote) have been identified and quantified at locations within the boundaries of the RAB Site.  Two
site samples (one soil, one water), collected by the Oklahoma State Department of Health in 1989 for a
Preliminary Assessment, indicated the presence of 617 mg/Kg (ppm) of lead, and five PAH compounds
(total concentration of approximately 52,000 mg/kg) in the soil sample.

The TSC was requested by the RPM to provide Field Screening support utilizing the Field-Portable
Scanning Spectrofluorometer (FPSS).  The principle contaminants are PCPs, PAHs, and Dioxins.

On-Site FPSS measurements and samplings of site soils and sediments were conducted during the second
quarter of  1995. The  data obtained from the FPSS will be used to define the levels and distribution of
the identified organic  contaminants. A report identifying the measurement results is in process.
 Project Name:  South Cavalcade
 Site: South Cavalcade SF Site
 Site ID: TXD980810386

 Type-Lead:
 Requested by:  Glenn Celerier (214) 665-8523
 Lead Scientist: A.K. Singh (702) 435-3731
Job Order No: 22601106
 Start Date: July 1994
 Expected Completion Date: January 1995
 Revised Completion Date: December 1995

 Estimated Budget: 57,000
 Revised Budget: 520,000
 Major Contaminants: Organics
 Total Expenditures: 516,311
 Total FY95 Expenditures: 512,571
 Total 3rd Qtr. Expenditures: 5813
 Beazer East, Inc. (BEI) representing the PRP(s) is implementing a Record of Decision issued for the
 South Cavalcade Superfund Site in Houston, Texas.  In July, the RPM requested a review of these
 statistical methods as described in Section 2.0 and Section 4.0 of "Draft Confirmational Sampling Plan
 (Dames & Moore, June 1994, REV 1)" for the South Cavalcade Superfund Site.
                                              15

-------
   The confirmational sampling plan outlines the overall sampling strategy and specific sampling and
   analysis procedures for the confirmation of the clean perimeter of the impacted areas, and for
   verification that impacted soils have been remediated in accordance with EPA guidance.

   CRD-LV TSC scientist(s) reviewed the appropriate sampling plan sections and provided the Regional
   RPM with suggestions and recommendations. CRD-LV TSC scientists participated in a negotiation
   meeting with the PRPs during the second and third quarters to discuss monitoring/sampling design
   approaches.
REGION 7
    Project Name:
    Site: Kem-Pest Laboratories SF Site
    Site ID: MOD980631113

    Type-Lead: Fund
    Requested by: C. Thigpen (913) 551-7414
    Lead Scientist: P. Fitzpatrick (702)  897-3379

    Start Date: December 1993
    Expected Completion Date: May  1994
    Revised Completion Date: December 1995

    Estimated Budget:  S25.000
    Revised Budget: S50,000
    Major Contaminants: Pesticides/Metals
Job Order No: 226 10189
Total Expenditures: 540,349
Total FY95 Expenditures: S 10,056
Total 3rd Qtr. Expenditures: S31
    The RPM requested that the TSC develop a site specific S&A Plan, analytical approach, and a QAPjP to
    determine if site contaminants have penetrated the walls and floor of the Formulation Building. The
    TSC provided the Sampling/Monitoring QA plan titled, "Quality Assurance Project Plan and Sampling
    Plan for the Kem-Pest Superfund Site Cape Girardeau County, Missouri", to the RPM.  The PRP's have
    reviewed the QAPjP/Sampling Plan. The Region has requested that the CRD-LV TSC provide on-site
    sampling support.  Efforts to address this request are currently in process. A delay in the on-site
    sampling effort has occurred. This TSC project is currently on hold.
 •  Project Name:  Lindsay Manufacturing Soil Partitioning
    Site: Lindsay Manufacturing SF Site
    Site ID:                                       Job Order No: 22401108

    Type-Lead: Fund
    Requested by:  Cecilia Tapia (913) 551-7733
    Lead Scientist: Marti Minnich (702) 897-3258

    Start Date: February 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

                                                  16

-------
   Estimated Budget: Sl2,000
   Revised Budget: S
   Major Contaminants: Organics
Total Expenditures: $7,979
Total FY95 Expenditures: 57,979
Total 3rd Qtr. Expenditures: S6,654
   The Regional RPM requested assistance in the determination of site-specific soil-water partition
   coefficients for the Lindsay Manufacturing Superfund site located in Lindsay, Nebraska. The partition
   coefficients will be used in the calculation of subsurface soil cleanup levels for the site.

   The CRD-LV TSC has selected a method that was specifically designed to measure soil-water
   partitioning of volatile organic compounds.  Five (5) soil samples have been collected and received from
   the site for this analysis.  Two of the samples were previously air-dried and sieved.  Three of the samples
   were moist.  The moist samples appeared very sticky and cohesive, indicating substantial clay contents.
   The soil sorption coefficient Kd for U.dichloroethene (1,1-DCE), 1,1,1-trichloroethane (1,1,1-TCA), and
   tetrachloroethene (PCE) was determined on all five samples. A report titled, "Soil K,, Determination for
   Lindsay Manufacturing Site", and the "raw" data was provided to the Region.
REGION 8
    Project Name: Utah Power/Light-American Barrel Site
    Site: Utah Power/Light-American Barrel SF Site
    Site ID:                                        Job Order No: 224 10186

    Type-Lead:
    Requested by: David Ostrander (303) 293-1530
    Lead Scientist: Neal  Amick(702) 897-3231
    Start Date: November 1993
    Expected Completion Date: June 1994
    Revised Completion Date: December 1995
    Estimated Budget: 525,000
    Revised Budget: S
    Major Contaminants: Organics
 Total Expenditures: S4,759
 Total FY95 Expenditures: S2,519
 Total 3rd Qtr. Expenditures: S67
    The RPM requested that the TSC provide field measurements using the Field Portable Scanning
    Spectrofluorometer (FPSS).  The measurements will be used relative to the excavation of contaminated
    soils and possibly for confirming sample analysis.  A field test of the FPSS was completed at the
    American Creosote NPL Site. The results of this field test (instrument performance) will be used in the
    development of an analysis and QA Plan for the  American Barrel Site. Site samples were sent to the
    CRD-LV TSC for instrument calibration purposes. Site samples have been analyzed and the data
    evaluated.  It is anticipated that field measurements will take place during the fourth quarter 1995.
 REGION 9

 •   Project Name: Allied Signal North Hollywood
     Site: Allied Signal SF Site
     Site ID:
 Job Order No:
                                                  17

-------
Type-Lead:
Requested by: Dave Setter (415) 744-2260
Lead Scientist: Alan Crockett (208) 526-1574/Jeff Sondrup (208) 526-8396

Start Date: June 1994
Expected Completion Date: March 1995
Revised Completion Date: December 1995

Estimated Budget: S30,000                       Total Expenditures: 525,970
Revised Budget: S                              Total FY95 Expenditures: 57,265
Major Contaminants:Organics                   Total 3rd Qtr. Expenditures: 57,265


The Region IX  RPM requested that the TSC provide assistance in evaluating the Allied Signal site as a
source of ground water contamination within the North Hollywood Operable Unit. Specifically, the TSC
evaluation will focus on the following:

•   Determine if Allied's soil gas investigation was performed using appropriate field and analytical
    methodology,

•   Perform an  independent  assessment of the data, and compare these findings with those made by
    Allied's contractor,

•   Determine whether the placement of probes was adequate to characterize source area, and

•   Identify data gaps and make recommendations as to whether additional work is necessary.

In addition, the  TSC will provide  assistance in determining if Allied's soil boring investigation was
performed using appropriate  field and analytical methodology, determine whether the placement of
borings was adequate to characterize source areas, attempt to determine whether the findings of the soil
boring study are consistent or inconsistent with the soil gas results, comment on the soil matrix data in
light of the subsurface conditions found, particularly address the likelihood that contaminant releases
would have a 'wandering' pattern  through  the subsurface, and identify data gaps and make
recommendations as to whether additional work is necessary.

In support of this effort, TSC scientist(s) provided  the document titled, "Review of Environmental
Characterization Data concerning the Allied Signal, Inc., North Hollywood Site, San Fernando Operable Unit,
San Fernando Valley,  California." A Conflict of Interest  (COI) problem as identified was resolved during
the second quarter of FY95. A meeting between Region 9, NEIC, INEL and CRD-LV personnel was
held to address  and identify further assessment needs.
 Project Name: Carson River Mercury
 Site: Carson River Mercury SF Site
 Site ID:                                       Job Order No: 224 10101

 Type-Lead:Fund
 Requested by: Sean P. Hogan (415) 744-2236
 Lead Scientist: David Dobb (702) 897-3273
                                              18

-------
Start Date: September 1993
Expected Completion Date: February 1994
Revised Completion  Date: September 1995
Estimated Budget:SlO,000
Revised Budget:
Major Contaminants: Mercury
Total Expenditures: $28,794, PC&B $2,500
Total FY95 Expenditures:S27,394, PC&B S1300
Total 3rd Qtr. Expenditures: S591, PC&B S600
The Regional RPM requested support from the CRD-LV TSC to perform mercury speciation analyses
on ten soil samples from the Carson River Mercury Site (CRMS).  As part of EPA's effort to
characterize mercury levels in soils at and around historic mill sites, the Region collected samples to
measure the levels of different mercury species (i.e., elemental mercury, mercuric sulfide, methyl mercury
and mercuric chloride) in the soil matrix. The purpose for acquiring these analytical data is to more
accurately characterize the human health risks associated with soils that have different mercury species
and different toxicity characteristics. The samples were analyzed and the results provided to the RPM.
For confirmatory purposes, additional analyses was performed. The RPM requested additional support in
developing a monitoring approach for the site. The results of additional analysis was provided to the
RPM. In addition, a preliminary sampling/monitoring design approach was provided to the RPM. The
CRD-LV TSC provided a geostatistical assessment of data  collected near Dayton.  A data assessment
explanation was provided to the RPM.
 Project Name: Concord Navel Weapons Station NPL Site
 Site: Concord Naval SF Site
 Site ID:                                       Job Order No:

 Type-Lead:Fund
 Requested by: Richard Freitas (415) 744-2315/Barbara M. Smith (415) 744-2366
 Lead Scientist: Alan Crockett (208) 526-1574/Bob Starr (208) 526-5687

 Start Date: March 1995
 Expected Completion Date: December 1995
 Revised Completion Date:
 Estimated Budget:S 12,000
 Revised Budget:
 Major Contaminants: Mercury (Heavy Metals)
 Total Expenditures: 53,320
 Total FY95 Expenditures: S3.320
 Total 3rd Qtr. Expenditures: $2,384
 The Naval Weapons Station Concord is in the north-central portion of Contra Costa County,
 approximately 30 miles northwest of San Francisco, California. The station operated an ocean terminal
 facility to transship ordnance from trucks or railcars to ships and vice versa. The base realignment and
 closure activities at other facilities in the west have made Concord a significant military ordnance and
 transshipment facility on the west coast.  The station encompasses nearly 13,000 acres.

 At the present time, RI work plans and field sampling plans for Tidal and Inland Areas have been
 submitted and approved by the Navy, State, and EPA.  Work will commence on these sites in April,
 1995.  The work plan for an Ecological Assessment of the Litigation Sites has been approved to evaluate
 the remaining effects of hazardous levels of heavy metals not previously removed by the Navy.  This work
 is also scheduled to begin in April, 1995.  Investigations of groundwater as a contaminant transport
 pathway into the Tidal Area Sites and Litigation Sites has been postponed, pending data  from soils,
 sediments, and surface water, and input from the CRD-LV TSC technical experts.

                                               19

-------
The evaluation and implementation of better approaches to address the question of groundwater as a
transport pathway for organic and inorganic contaminants in wetland soils and sediments is a significant
technologic gap in the investigation of wetland sites at Concord. The CRD-LV TSC is currently
reviewing available site data. A recommended sampling approach was provided to the Region.
Project Name:  King Tut Superfund Site
Site: King Tut SF Site
Site ID:
Job Order No: INEL
Type-Lead:
Requested by: Richard Lessler (415) 744-1063/Patti Collins (415) 744-2229
Lead Scientist: Alan Crockett (208) 526-1574/Richard Wells (208) 526-4561 INEL

Start Date: May 1995
Expected Completion Date: September 1995
Revised  Completion Date:
 Estimated Budget: S2,000
 Revised Budget: S
 Major Contaminants: Radionuclide
 Total Expenditures: S100
 Total FY95 Expenditures: S100
 Total 3rd Qtr. Expenditures: $100
 This Regional request involved a review and making recommendations pertaining to analytical methods
 for the analysis of water, soils, and sediment samples for total thorium and uranium alpha particle
 activity. The requirements needed by the Region included a detailed standard operating procedure(s)
 explaining how the samples are to be handled and analyzed, and what quality control measurements and
 quality assurance procedures should be implemented.

 The TSC reviewed the analytical methods and provided recommendations and suggestions to the
 Regional Project Officer.
 Project Name:  Mare Island Data Audit
 Site: Mare Island SF Site
 Site ID:

 Type-Lead:
 Requested by: Stephen Remaley (415) 744-1496
 Lead Scientist: Mary Wolf (702) 897-3384

 Start Date: November 1994
 Expected  Completion Date: March 1995
 Revised Completion Date: September 1995

 Estimated Budget: S10,000
 Revised Budget: S
 Major Contaminants: Inorganics/Organics
 Job Order No: 224 01103
 Total Expenditures: $3,931, PC&B $300
 Total FY95 Expenditures: $3,931, PC&B $300
 Total 3rd Qtr. Expenditures: $67, PC&B $300
  The TSC was requested to conduct an audit of raw data generated by the analysis of samples collected at
  the Mare Island Superfund Site.  The audit of these data will focus on authenticating laboratory
  adherence to the principles of good laboratory practice in reporting results for compounds with
  contractual criteria.  The audit will address laboratory results for calibrations (criteria compounds),

                                               20

-------
   surrogates, internal standards areas, and tuning compound results.  The audit was completed during the
   second quarter FY95. Additional data audit explanations were provided to the Region.


•  Project Name:  Mather AFB Data Audit
   Site: Mather AFB SF Site
   Site ID:                                       Job Order No: 226 10106

   Type-Lead:
   Requested by: Debbie Lowe (415) 744-1490/Matt Hagemann (415) 744-2326
   Lead Scientist: C. Davis
    Start Date: December 1994
    Expected Completion Date: March 1995
    Revised Completion Date: September 1995

    Estimated Budget: S5,000                       Total Expenditures: S510
    Revised Budget: S                              Total FY95 Expenditures: S510
    Major Contaminants: Organics/Inorganics         Total 3rd Qtr. Expenditures: SO

    The Region's Hydrogeologist and the Remedial Project Manager requested that the TSC review Section
    3.2 of the "Draft 1994 Groundwater Monitoring Program Evaluation Report, Mather Air Force Base
    California."  The review and subsequent comments and suggestions will address the validity of the
    coefficient of variation  test to determine the "statistical predictability" as proposed by the Air Force.

    A report titled, "Review of Section 3.2 of the Draft 1994 Groundwater Program Monitoring Evaluation
    Report, Mather Air Force Base California" was prepared and submitted to the RPM. Additional  reviews
    of PRPs suggested approaches are anticipated.


    Project Name: McCormick-Baxter Wood-Treating Plant
    Site: McCormick-Baxter Wood-Treating SF Site
    Site ID:                                      Job Order No: 222 01 111
    Type-Lead:

    Requested by: Marie Lacy (415) 744-2234
    Lead Scientist: Joe R. Donnelly (702) 897-3387/Wayne Sovocool (702) 798-2212

    Start Date: March 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: S10,000                      Total Expenditures: $9,454
    Revised Budget: S                              Total FY95 Expenditures: S9,454
    Major Contaminants: Creosote                  Total 3rd Qtr. Expenditures: S8,910


     The McCormick and Baxter Wood-Treating site is  nine acres in size located in a light industrial area
     near the Port of Stockton.  From 1942 to 1990, utility poles and railroad ties were treated with creosote,


                                                 21

-------
pentachlorophenol (PCP), and arsenic compounds.  Waste oils generated from the wood-treatment
process were disposed of on site in unlined pools and concrete tanks.

The RREL Technical Support Center will test a remediation strategy in or after April 1995 at this site.
The process involves thermal desorption at 800° followed by bicarbonate, carbonate, and/or oxide
treatment of the organics to dechlorinate them.  RREL will run a ten day test, with slightly different
experimental conditions each day. The  contaminants are expected to be creosotes, pentachlorophenols
(PCPs), and trace-level dioxins.  Chromium-copper-arsenic catalyst may also be present.

The TSC was requested by the RPM  to provide  Field Screening support utilizing the Field-Portable
Scanning Spectrofluorometer  (FPSS). The principle contaminants are PCPs, PAHs, and Dioxins.

On-Site FPSS measurements and samplings of site soild and sediments were conducted. The data
obtained from the FPSS will be used  to define the levels and distribution of the identified organic
contaminants. A report identifying the measurement results is in process.


Project Name:  Modesto Groundwater  Superfund Site
Site: Modesto SF Site
Site  ID:                                        Job Order No:
Type-Lead:

Requested by: John Lucey (415) 744-2222
Lead Scientist:  Alan Crockett (208)  526-1574, Bob Starr (208) 526-5687 Greg Hulet (208) 526-0283

Start Date: December 1994
Expected Completion Date: September 1995
Revised Completion Date: December 1995


Estimated Budget:  550,000                      Total Expenditures: 542,453
Revised Budget: S                              Total FY95 Expenditures: 542,453
Major Contaminants: Radionuclides/Organics     Total 3rd  Qtr. Expenditures: 545

The Regional RPM requested technical support for the Modesto Groundwater Contamination Superfund
Site located in Modesto, California.  The Site consists of a dry cleaner facility which leaked PCE
contamination into the soil and  groundwater.  It was recently discovered that the groundwater is also
contaminated with naturally occurring  uranium. EPA has performed an RI/FS at the site and selected a
 preferred cleanup alternative which consists of pump and treat with GAC for groundwater
 contamination, and SVE for soil contamination. The FS will now have to be revised to evaluate
 remedial technologies for the cleanup of radiation related to the naturally occurring uranium.

 The objective of this technical support effort is to assist the RPM in selecting  the most reliable, efficient
 and cost effective remedial technologies to clean up the site.  The following three areas are being
 addressed by the CRD-LV TSC:

 •   Identify data gaps in existing data  and  recommend  additional data requirements. The groundwater,
     soil, and soil gas, were tested for many different parameters during the RI.  Besides uranium the
     groundwater was also tested for  gross alpha, gross beta, and radium. The soil-soil gas was not
     analyzed for radiation.
                                               22

-------
    •    Identify potential radiation remedial technologies. There are several remedial technologies (or
        combination of technologies) which could be utilized for groundwater remediation at the site.
        Potential technologies including reverse osmosis, ion exchange, air stripping, and granular activated
        carbon (GAC).

    •    Prepare site cleanup cost estimate for each appropriate technology. After the appropriate
        technologies are identified a cost estimate will be prepared.

    In support of this effort the CRD-LV TSC has provided, "Recommended Data Acquisition for the
    Modesto Groundwater Contamination Site" and the report, "Treatment Alternatives Report Modesto
    Groundwater Contamination  Site." The RPM is currently reviewing these documents. A site visit to audit
    sampling procedures is anticipated  for the fourth quarter.


•   Project Name:  Montrose DDT Superfund Site
    Site: Montrose SF Site
    Site ID:                         Job Order No: 224 10106

    Type-Lead:
    Requested by. Dan Shane (415) 744-2286
    Lead Scientist: Mobile Laboratory

    Start Date: May 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: 51,000                       Total Expenditures: S747
    Revised Budget: S                              Total FY95 Expenditures: S747
    Major Contaminants:                           Total 3rd Qtr. Expenditures: $747

    The Regional On-Scene Coordinator requested that the CRD-LV TSC measure site contaminants using
    an on-site mobile laboratory.  This request involved utilizing the T04 air sampling method(s) with GC
    ECD analysis.  The TSC recommendation(s) was that this method was not suitable for an on-site mobile
    laboratory application.  The rational  for this assessment was that the analytical method required a 12
    hour soxhlet extraction, a 23  hour sample turn-a-round time could be expected, and this procedure
    requires the  use of 5% ether  in Hexane which is extremely flammable and required the use of a
    specialized laboratory hood.  This information with analytical alternatives was provided to the Region.


•   Project Name: Phelps Dodge Douglas Reduction Works ESI/RI
    Site: Phelps Dodge SF Site
    Site ID:                         Job Order No: 224 10199

    Type-Lead:
    Requested by: Michael E. Bellot (415) 744-2243/Kira  Lynch (510) 412-2334
    Lead Scientist: Conrad Kuharic (702) 897-3246/Danny Jackson

    Start Date: October 1994
    Expected Completion Date: September 1995
    Revised Completion Date:
                                                 23

-------
   Estimated Budget: S20.000                      Total Expenditures: 59,535
   Revised Budget: S                              Total FY95 Expenditures: S9,535
   Major Contaminants: Metals                    Total 3rd Qtr. Expenditures: SO

   The TSC was requested to review site documents (i.e., QAPjP, S&A Plan) and provide on-site support
   for measuring the levels and distribution of metal contamination. The sites ESI/RI was developed to
   determine if smelter emissions have impacted nearby communities.  X-Ray Fluorescence will be used,  if
   appropriate, to measure metal contaminants.

   Specifically the TSC will provide:

   •   A quick turn-around review of the proposed XRF procedures,

   •   Identifying analytical methods that are capable of "fingerprinting" lead from specific sources,

   •   Review of suggested  investigation plan approaches,

   •   Field support for XRF calibration and implementation,

   •   Remote sensing applications, and

   •   Monitoring design and data assessment.

   A report that addresses the TSC review of available site documents was prepared and submitted to  the
   Region. This project is currently on  hold.


•  Project Name: San Fernando Valley Basin (SFV)
   Site: San Fernando SF Site
   Site ID:                        Job  Order No:

   Type-Lead:
   Requested by: Ned Black (415) 744-2253
   Lead Scientist A.K. Singh (702) 435-3731

   Start Date: October 1994
   Expected Completion Date: September 1995
   Revised Completion Date:

   Estimated Budget: S5,000                       Total Expenditures: PC&B, $300
   Revised Budget: S                              Total FY95 Expenditures: PC&B, $300
    Major Contaminants: Organics                  Total 3rd Qtr. Expenditures: PC&B, S300
                                                  (No TSC Resources were utilized)

    Four sites are within the San Fernando Vally (SFV) for inclusion on the National Priority  List (NPL):
    North Hollywood, Crystal Springs, Pollock, and Verdugo. Currently, EPA is managing the four areas as
    one large site referred to as the SFV Superfund Site. This site includes the four NPL sites and adjacent
    areas where groundwater contamination is known or presumed to  have migrated.  There  are currently a
    total of 87 RI monitoring wells located inland adjacent to the  four NPL sites.  Three of the shallow
    water table wells are screened in bedrock and do not have pumps installed. Trichloroethylene (TCE) and
    tetrachloroethylene (PCE) data were used to separate the 84 RI wells into two categories:  those
                                                 24

-------
    recommended to be sampled quarterly, and those recommended to be sampled annually.  All 84 of the
    RI wells were originally included in the annual monitoring program. Of these 84 wells, 41 historically
    having concentrations of TCE and/or PCE in excess of federal and state maximum contaminant levels
    (MCLs) were placed into the quarterly monitoring program.

    The Region is concerned with both PCE and TCE as contaminants in the groundwater. It has been
    suggested that krieging using plume maps might be a good way to access changes in contaminant
    concentrations over time. In addition, the Region is interested in any other means of characterizing
    migration of the contaminant plumes or changes in contaminant concentrations over time which seem
    pertinent.

    The CRD-LV TSC reviewed the provided data and identified a number of data assessment methods that
    could be used to assess contaminant behavior over time.
REGION 10
    Project Name: ASARCO Smelter Superfund Site
    Site: ASARCO Smelter SF Site
    Site ID:                        Job Order No: INEL

    Type-Lead:
    Requested by: Bernard Zavala (206) 553-1562
    Lead Scientist: Glen Carpenter (208) 526-4166

    Start Date: June 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: S2,000                       Total Expenditures: S100
    Revised Budget: S                             Total FY95 Expenditures: $100
    Major Contaminants: Organics                  Total 3rd Qtr. Expenditures: $100 INEL

    The Regional Groundwater Forum  requested that the CRD-LV TSC review the adequacy of changing a
    proposed seismic velocity survey from a "cross-hole" configuration to a "surface to borehole"
    configuration. The TSC reviewed the geophysical approach(s) and provided recommendations to the
    region.
    Project Name:  Bunker Hill
    Site: Bunker Hill SF Site
    Site ID: IDD048340921                        Job Order No: 224 10198

    Type-Lead:
    Requested by: Greg Gervais (206)553-1906/Danny Jackson (702) 897-3245
    Lead Scientist: Russ  Plumb (702) 897-3265

    Start Date: September 1994
    Expected Completion Date: September 1995
    Revised Completion  Date: January 1996
                                                25

-------
Estimated Budget: 525,000
Revised Budget: $35,000
Major Contaminants: Inorganics
              Total Expenditures: S20,841
              Total FY95 Expenditures: 520,441
              Total 3rd Qtr. Expenditures: $6,360
The Region X Project Officer requested that approaches be examined to determine whether the Bunker
Hill site characterization techniques have been addressed sufficiently:  A sampling/monitoring approach
for confirming the vertical and lateral extent of soil/sediment contamination, procedures for identifying
levels of soil, sediment, and possibly water contamination, the quality assurance/quality control (QA/QC)
plan, the S&A plan and all other methods that have been used to fully characterize the site for remedial
purposes.   In addition, an assessment of data needs necessary to satisfy the characterization objectives
will be.required if past characterization efforts have not adequately characterized the sites contaminants.
This data  assessment will involve data interpretation and recommendations involving statistical and other
tests necessary for making decisions concerning the extent of site contaminants.

This technical support project will increase the knowledge of how  to assess impacts on local
hydrology/geology for the tailings.  This effort is critical not only to site characterization and to
development of monitoring strategies for detecting pollution, but also for contributing to appropriate
corrective action programs.  Also,  this effort will integrate saturated and unsaturated zone monitoring,
and site characterization methods  used in developing a monitoring well and sampling network design at
mine sites. Assessing site documents and data is in process. A number of recommendations pertaining to
the monitoring design and data  assessment was provided to the Region.
 Project Name: Lyman Mining
 Site: Lyman Mining SF Site
 Site ID:
Job Order No: 22401100
 Type-Lead:
 Requested by: Harry Craig (503) 326-3689
 Lead Scientist: Ed Heithmar (702) 798-2626/David Dobb (702) 897-3273

 Start Date: October 1994
 Expected  Completion Date: February 1995
 Revised Completion Date: September 1995
 Estimated Budget: 520,000
 Revised Budget: 5
 Major Contaminants: Mercury
               Total Expenditures: $9,651
               Total FY95 Expenditures: $9,651
               Total 3rd Qtr. Expenditures: $13
 The TSC was requested by the Regional RPM to analyze fourteen soil samples collected from the Lyman
 Mining site for individual mercury species.  The determination of mercury species is via an analytical
 method developed by CRD-LV.  The method separates mercury and mercury compounds into five
 difference species: Organic (e.g., Ch3HgCl), water soluble (e.g., HgCU), acid soluble (i.g., HgO and
 HgS04), metallic (HgO and amalgams), and mercury sulfide (HgS).

 During November, the TSC received and analyzed the samples from the Lyman Mining site. Following
 the analysis and assessment of the resulting data, a report was written and  provided to the requesting
 RPM. Oregon State employee's  required additional  explanation  on a number of items in the data report.
 The TSC provided clarification of these items.
                                                26

-------
                         SUPERFUND SHORT-TERM REQUESTS
Project Name:  Short Term Requests
Site: Short Term Requests
Site ID:
                               Job Order No: 224 10106
Type-Lead:
Requested by: See Below
Lead Scientist: TSC/CRD-LV Staff Scientists

Start Date: October 1991
Expected Completion Date: September 1995
Revised Completion Date:

Estimated Budget: 5150,000
Revised Budget: 5200,000
Major Contaminants: Variable
Total Expenditures: $225,112
Total FY95 Expenditures: S25,454
Total 3rd Qtr. Expenditures: S6,317
 TSC requests that can be completed within a 40-hour period:
-
REGION
STATE
=====
3

9
1
3
2
4
9
Hdq
g
2
2
3
1
8
1
DATE
===
April
April
April
May
June
May
June
June
May
June
June
May
April
April
May
1
SITE
_—
Issue Paper


Western Sand
Aberdeen Proving
Mercury Refining
Aberdeen Dumps
Allied Signal

Allied Signal
Koppers
Koppers
Morgantown
Pownel
Amer. Barrel
REQUESTOR
=====
F. Vavra
J. Holland
B. Gore
A. Klinger
D. loven
M. O'Brian
K. Crane
D. Setter
R. Landy
S. Sisk
L. Mareno
K. Kowalski
M. Whittington
T. Connelly
D. Ostrander
1
TELEPHONE
NUMBER
==========
(215)597-0676
(515)294-5839
736-5757
(617)573-9662
(215)597-1309
(505)881-2338
(404)347-3555
(415)744-2260
(410)573-6855
(303)236-5136
(215)597-0985
(215)619-4129
(215)597-1286
(616)573-9638
(303)293-1530
=====
NATURE OF
REQUEST
==============
Sampling
Immunoassay
Sampling
Data Assessment
Analysis
Data Assessment
Sampling
RARE
Sampling
Sampling
Sampling
Data Assessment
Analysis
Analysis
                                             27

-------
REGION
STATE
5
2
6
9
5
1
3
9
5
9
9
5
9
1
1
5
4
4
2
RREL
9
USDOE
USDOE
3
9
5
9

DATE
May
April
May
May
June
May
May
May
May
April
May
May
June
May
April
May
May
May
April
May
May
May
June
April
April
April
May
April
SITE
Ironton Coke
Passaic River

Edwards AFB
Ironton Coke
W.R. Grace
Altantic Wood
Montrose
Lorain County

Montrose
Lorain County

O'Connor
O'Connor
Brownfields
Escambia
Escambia
NARPM's
Brownfields



Navy Ships
McCormick
No.Dr./Oak Street
Concord

REQUESTOR
T. Alcamo
J. Josephs
L. Ross
R. Russell
T. Alcamo
L. Jennings
D. lacono
D. Shane
S. Renninger
M. Bellot
R. Randle
M. Murphy
J. Ricks
J. Griswald
R. Gilleland
W. Messenger
G.Linder
M Fite
S. Jaffess
F. Freestone
R. Simm
D. Page
G. Carpenter
A. Sochanski
M. Lacey
R. Ellison
B. Smith
S. Coulter
TELEPHONE
NUMBER
(312)886-7278
(212)637-4317
(214)665-6665
(415)744-2406
(312)886-7278
(617)573-9634
(215)597-8445
(415)744-2286
(216)323-9540
(415)744-2243
(310)435-6180
(216)322-7513
(415)744-2402
(603)224-7979
(617)573-5766

(904)488-0190
(404)347-2643
(212)637-4340
(908)321-6632
(415)744-2360
(615)564-8922
(208)526-4166
(215)597-3167
(415)744-2234
(313)692-7269

263-3136
NATURE OF
REQUEST
Analysis
Dioxin
Sampling
Analysis
Analysis
Data Assessment
Analysis
Analysis
Analysis
Sampling
Analysis
Analysis
Sampling
Data Assessment
Data Assessment
Monitoring
Analysis
Analysis
Conference
Sampling
Analysis
Workshop
Geophysics
Monitoring
Analysis
Analysis

Sampling
28

-------
                                  RCRA CORRECTIVE ACTION
REGION 1
    Project Name: Envirite RCRA Facility
    Site: Envirite RCRA Facility
    Site ID:

    Type-Lead:
    Requested by: Ray Cody (617) 573-5769
    Lead Scientist: Danny Jackson (702) 897-3245 (702) 897-3245

    Start Date: May 1995
    Expected Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: S7,000
    Revised Budget: S
    Major Contaminants: Synthetic Acid Precipitation
        Job Order No: 226 10602
        Total Expenditures: S2.207
        Total FY95 Expenditures: $2,207
        Total 3rd Qtr. Expenditures: 52,207
    The Regional RCRA Project Officer requested that the CRD-LV TSC evaluate using the Synthetic
    Precipitation Leaching Procedure (SPLP) in lieu of the Toxicity Characteristic Leaching Procedure
    (TCLP) to determine the capacity for landfilled sludges to leach contaminants.  The SPLP is similar to
    the TCLP but the initial liquid-solid separation step had been eliminated and the acetate buffer
    extraction fluid has been replaced by a dilute nitric acid/sulfuric acid mixture.

    In summary, the Region required information pertaining to the following:

     •   What is the specific chemical composition (topical) of the metal-hydroxide sludge?  How are the
         metals bound to the inorganic matrix?

     .   What is the efficiency of the metal-hydroxide production process? Are there more than one
         species of a given  metal?

     .   Does there happen to be literature which depicts the  stability of the predominant form(s) of
         metal/binder species as  a function of pH?

     The TSC addressed the required issues and provided the Region with suggestions and
     recommendations.
 REGION 5

 •   Project Name:  Columbus Solid Waste Reduction
     Site: Columbus Waste-To-Energy RCRA Facility
     Site ID:
Job Order No: 222 10609
     Type-Lead:
     Requested by: Carole T. Braverman (312) 886-2910
     Lead Scientist: A. K. Singh (702) 435-3731/Vicki Ecker (702) 897-3223
                                                 29

-------
Start Date: March 1995
Expected Completion Date: September 1995
Revised Completion Date:

Estimated Budget: 510,000                       Total Expenditures: S 13,533
Revised Budget: 518,000                                   Total FY95 Expenditures: $13,533
Major Contaminants:Dioxin                     Total 3rd Qtr. Expenditures: 512,894

The Columbus municipal Electric Utility Boiler, also known as the Columbus Municipal Electric Plant
(CMEP), is located south of downtown Columbus, Ohio.  The facility is a power generating plant
fueled by coal and refuse.  It has been in operation since 1983 and is owned and operated by the City
of Columbus.

In 1987, the US EPA initiated a study of the incinerator ash at CMEP because of the presence of
dioxin and furan isomers associated with incinerator ash.  The special study report indicated that
incinerator ash contains dioxin and furan isomers, lead and cadmium. Concentrations of dioxin and
furan isomers range from 0.33 ppb to 2.13 ppb. The highest  concentrations were found in top ash
from  a conveyor belt. A relatively high concentration (0.84 ppb) was found from a stack scape sample.
Dioxins (up to 0.38 ppb) were also found in two areas in the soil where ash was allowed to
accumulate.  Lead in the ash was found to exceed EP toxicity limits.

The Regional Risk Assessor has requested that the CRD-LV TSC design a sampling/monitoring
strategy and a quality assurance project plan that would identify the concentration of soil dioxins. The
soil dioxin concentrations that are of interest  are 20, 40, 70 and  100 ppt.  The CRD-LV TSC  is in the
process of designing a sampling/monitoring program and finalizing the quality assurance project plan.


Project Name: Metalworking Lubricants (MWL)
Site:  Metalworking Lubricants RCRA Facility
Site ID: IND 000 646 950                       Job  Order No: 224 10610

Type-Lead:
Requested by:  Tamara Lamm (312) 886-0991
Lead Scientist: Danny Jackson (702) 897-3245 (702) 798-3295

Start Date: March 1995
Expected Completion Date: September 1995
Revised Completion Date:

Estimated Budget: S6,000                        Total Expenditures: $479
Revised Budget: S                               Total FY95 Expenditures: S479
Major Contaminants: Dioxin                     Total 3rd Qtr. Expenditures: $479

The Metalworking Lubricants facility is located in Indianapolis,  Indiana.  The facility currently
processes waste oils from various metalworking, automotive, and steel mill manufacturing facilities.
 Waste oils are processed and blended using batch processes,  and specification oils are returned to the
client industries. RCRA regulated waste streams are not generated by any of the processing or
blending operations. Land use surrounding the facility is largely industrial. To the west, the Indiana
 Railroad  (formerly Illinois Central & Gulf) operates a  rail siding area utilized as  a locomotive and rail
 car scraping yard. Land to the south and east is undeveloped made land.  An active filling operation
 is occurring on the property immediately to the south,  and grades in this area have been raised several
 feet.  Land to  the north was formerly the site of a salvage yard.

                                              30

-------
   Because of the types of materials that have been used at the facility, the Regional Project Manager
   believes that the target list for the RFI should include dioxins and furans.  The CRD-LV TSC
   reviewed facility documents and data. An initial report with CRD-LV TSC recommendations was
   provided to the RCRA Project Officer.
REGION 8


.   Project Name: EXXON Billings Refinery
    Site: EXXON Refinery RCRA Facility
    Site ID.                                       Job Order No: 226 10611

    Type-Lead:
    Requested by: Stephanie Wallace (406) 449-5414 Ext 227
    Lead Scientist: Neal Amick (702) 897-3231

    Start Date: June 1995
    Expected  Completion Date: September 1995
    Revised Completion Date:

    Estimated Budget: S8,000                        Total Expenditures: SO
    Revised Budget: S                              Total FY95 Expenditures: SO
    Major Contaminants: PAHs                     Total 3rd Qtr. Expenditures: SO

    The Region  is currently over-seeing a facility investigation at the EXXON Refinery. The objective(s)
    of this investigation are to identify and determine if waste constituents have  affected soil or
    groundwater quality and to summarize the nature and geophysical extent of any affected soils and/or
    groundwater.

    The CRD-LV has been requested to assist in this effort by measuring the levels of PAHs in sampled
     media usine the Field-Portable Scanning Spectrofluorometer. The measurements will be made during
     the fourth quarter of FY95.  Following the on-site measurements, a  report identifying the samples
     analyzed  and the results obtained will be submitted.
  REGION 9

  •  Project Name:  GTE
     Site: GTE RCRA Facility
     Site ID.                                      Job Order No: 222 95611

     Type-Lead:
     Requested by: Frank Gardner (415) 744-2039
     Lead Scientist: Dave Williams

     Start Date: September 1994
     Expected Completion Date: January 1995
     Revised Completion Date:  September 1995
                                                  31

-------
Estimated Budget: 31,000                       Total Expenditures: $8,213
Revised Budget: S8.500                         Total FY95 Expenditures: S8,213
Major Contaminants: Organics/Inorganics         Total 3rd Qtr. Expenditures: S339


The Region IX Project Officer requested that the CRD-LV TSC obtain available remote sensing
(photographs) documentation, and provide an assessment of this information for identifying
operations, determining waste management practices of the facility operators and to help locate
contaminant sources. Only archival photography will be required. The existing photography will
represent the years 1930's through the present.

The GTE facility is a manufacturer of communications equipment and has occupied an approximately
70 acre site in Silicone Valley since the early 1950's.  Available photographs were received.
Assessment of these photographs was completed.  The remote sensing report titled, "Aerial
Photographic Analysis  of GTE Government Systems", was provided to the Region.


Project Name: Gosford Lease/Former Magna Facility
Site: Magna RCRA Facility
Site ID:                                       Job Order No:  222 10608

Type-Lead: RCRA
Requested by: Ron Leach (415) 744-2031
Lead Scientist: D. Jackson  (702) 897-3245

Start Date: February, 1995
Expected Completion  Date: September 1995
Revised Completion Date:

Estimated Budget: S5,000                       Total Expenditures: S 1,467
 Revised Budget: S                              Total FY95 Expenditures: 51,467
 Major Contaminants: Petroleum Hydrocarbons    Total 3rd Qtr. Expenditures: S207


 The Magna Facility is  a 1.5 acre site in Bakersfield, CA with soil contamination. The contamination is
 very acidic refinery waste containing petroleum hydrocarbons, VOCs, SVOCs and sulfur compounds.
 The waste was deposited in the 1940s by Agri-Chem, a now-defunct lessee of the current property
 owner, Southern Pacific Transportation Company. There is no current information pertaining to the
 business practices and processes at Agri-Chem in the 1940s.

 A Corrective Measure Study (CMS) approach for the Magna facility has been prepared.  The Regional
 Project Officer (RPO) has requested that the CRD-LV TSC review the CMS report to determine if
 the suggested approaches are appropriate.  The TSC provided the Region a report titled, "Te.nnical
 Support Review of Corrective Measures Study Gosford Lease/Former Magna Facility", dated February
 14, 1995.
                                             32

-------
    Project Name: Quemetco Facility
    Site ID: Quemetco RCRA Facility

    Type-Lead:
    Requested by: Frank Gardner (415) 744-2039
    Lead Scientist: Dave Williams (702) 897-3390
Job Order No: L12 95610
    Start Date: September 1994
    Expected Completion Date: January 1995
    Revised Completion  Date: September 1995

    Estimated Budget: S7,000
    Revised Budget: S9,000
    Major Contaminants: Organics/Inorganics
Total Expenditures: 58,707
Total FY95 Expenditures: S8,707
Total 3rd Qtr. Expenditures: S701
The Region IX Project Officer requested that the CRD-LV TSC obtain available remote sensing
(photographs) documentation, and provide an assessment of this information for identifying operations,
determining waste management practices of the facility operators and to help locate contaminant sources.
Only archival photography will be required. Available photographs are currently being identified.

The Quemetco, Inc. facility is a secondary lead smelter that recycles lead-acid batteries and is located in
the Los Angeles,  California area. Historic facility operations such as  outdoor slag piles, a surface
impoundment, and a battery crusher have contaminated both on-site and off-site soils with lead.  Recently,
a former dry well was discovered, indicating that the Region may not yet have a complete data  base as to
past operations at this facility. Since the area has been used for industrial activities since the early 1950's
and recent construction in the area have altered the site's layout.  Available  photographs dating back to
the 1930's was required  for this remote sensing assessment.  Available photographs have been identified
and received.  Assessment of these photographs was completed. The  final Quemetco remote sensing report
was provided to the Region.
                                                 33

-------
                            RCRA SHORT TERM REQUEST
Project Name:  Short-term RCRA Technical Support
Site: Short Term RCRA Technical Support
Site ID:

Type-Lead:
Requested by: See below
Lead Scientist: CRD-LV/TSC Staff Scientists

Start Date: October 1, 1991
Expected Completion Date: September 1995
Revised Completion Date:

Estimated Budget: 58,000
Revised Budget: S40,000
Major Contaminants:
Job Order No: 226 10602
Total Expenditures: S40.140
Total FY95 Expenditures: S 1,439
Total 3rd Qtr. Expenditures: 51,414
TSC requests that can be completed within a 40-hour period. See request below:
REGION
8
8
1
5
5
1
4
4
DATE
May
May
June
April
April
April
April
May
SITE
Exxon
Exxon
Envirite
Columbus

Vermont
General Compound

REQUESTOR
K. Canfield
S. Wallace
R. Cody
C. Braverman
T. Lamm
K. Jamison
D. Gerard
K. Wischkaemper
TELEPHONE
NUMBER
(406)245-7600
(406)449-5414
(617)573-5769
(312)886-2910
(312)886-0991
(802)241-3831
(813)971-3882
(404)347-3866
NATURE OF
REQUEST
Analysis
Tech Support
Data Assessment
Sampling
Sampling
Dioxin
GC-FTIMS
Tech Support
                                             34

-------
                     SUPERFUND REMOTE SENSING SHORT TERM REQUEST
•  Project Name: Remote Sensing
   Site:  Superfund  Short Term Remote Sensing Technical Support
   Site ID:

   Type-Lead:
   Requested by: See below
   Lead Scientist: CRD-LV/TSC Staff Scientists

   Start Date: 1993
   Expected Completion Date: September 1995
   Revised Completion Date:

   Estimated Budget: 520,000
   Revised Budget: S30,000
   Major Contaminants:
                                                       Job Order No: 221 95755
Total Expenditures: 525,594
Total FY95 Expenditures: 5978
Total 3rd Qtr. Expenditures: S661
   TSC Remote Sensing requests that can be completed within a 40-hour period. The CRD-LV TSC is
   requested to provide Remote Sensing support that requires a quick-turn-around time.  Projects that may
   be addressed within this 40 hour time frame include:

        •     The use of Geographic Information Systems (CIS) for site characterization.

        •     Providing plots of geostatistical related data for site characterization.

        •     Review of RI/FS reports and workplans, pertaining to the use of multi-spectral scanner,
              remote sensing and GIS technologies.

        •     Review of identification and  technological techniques and methods used in remote sensing
              site assessment.

        •     Providing expert testimony, coordinating and/or contributing to the validity and authenticity of
              "remote sensing" data used in cost recovery cases.
REGION
2
9
DATE
May
June
SITE


REQUESTOR
T. Bragalia
S. Hogan
TELEPHONE
NUMBER
(617)536-1876
(415)744-2236
NATURE OF
REQUEST
Photographs
Photographs

-------
                     RCRA REMOTE SENSING SHORT TERM REQUEST
Project Name: Remote Sensing
Site: RCRA Short Term Remote Sensing Technical Support
Site ID:

Type-Lead:
Requested by: See below
Lead Scientist: CRD-LV/TSC Staff Scientists

Start Date: 1993
Expected Completion Date: September 1995
Revised Completion Date:

Estimated Budget: $20,000
Revised Budget: S30.000
Major Contaminants:
Job Order No: 221 95615
Total Expenditures: S742
Total FY95 Expenditures: S742
Total 3rd Qtr. Expenditures: S232
TSC Remote Sensing requests that can be completed within a 40-hour period. The CRD-LV TSC is
requested to provide Remote Sensing support that requires a quick-turn-around  time. Projects that may
be addressed within this 40 hour time frame include:

     •     The use of Geographic Information Systems (GIS) for site characterization.

     •     Providing plots of geostatistical related data for site characterization.

     •     Review of RI/FS reports and workplans, pertaining to the use of multi-spectral scanner,
           remote sensing and  GIS technologies.

     •     Review of identification and technological techniques and methods used in remote sensing
           site assessment.

     •     Providing expert testimony, coordinating and/or contributing to the validity and authenticity of
           "remote sensing" data used in  cost recovery cases.
REGION
4
DATE
June
SITE
Columbus WTE
REQUESTOR
C. Braverman
TELEPHONE
NUMBER
(312)886-2910
NATURE OF
REQUEST
Photographs
                                             36

-------
                                           ISSUE PAPER
Project Name: Identifying Background
Site: Identifying Background
Site ID:

Type-Lead: Frank Vavra (215) 597-0676
Requested by: Engineering Forum
Lead Scientist:  Bob Breckenridge (208) 526-0757, Alan Crockett (208) 526-1574

Start Date: March 1993
Expected Completion Date: July 1994
Revised Completion Date:  September 1995
Estimated Budget: S25.000
Revised Budget:S30,000
Major Contaminants: Metals
Total Expenditures: S39,218
Total FY95 Expenditures: 512,660
Total 3rd Qtr. Expenditures: Si3,258
Background:  Many states have developed requirements for cleanups that are more stringent than risk based levels
and sometimes to background levels. The variability of naturally occurring inorganics may lead Federal/state
representatives to conclude that an area of a site has elevated metals just because of this variability. Establishment
of background based both on site specific sampling and comparison to normal background ranges can  help resolve
this issue.  Additionally, Natural Resource Trustees may request/require remediation of streams to levels below
typical background levels of man-made substances in developed areas.  Areas near roads usually have elevated
levels of lead from leaded gasoline, elevated levels of PAHs from exhaust and asphalt road material, elevated levels
of zinc from oxidation of car metals and elevated levels of inorganics from road salt/ashes. These contaminants are
washed into ditches near the road and accumulate with time.  Sites that were used as farmland may have elevated
levels of pesticides and inorganics from fertilizers and pesticides.  For example, lead arsenate was  the pesticide of
choice for orchards at one time in the past and fertilizers often contain lead which can accumulate in soils.
Identification of representative background levels is often difficult and is complicated by the presence of roads,
farms or other land use.

The CRD-LV TSC was requested by the  Engineering Forum to develop a standard process/procedure  to identify
background levels of naturally occurring inorganics and typical levels of man-made substances in soils and
sediments that may also be site contaminants.  The goal is to produce an issue paper that identifies critical
elements that must be taken to obtain representative background levels and the available processes that can assist
in this determination. Existing documents and sources of information will be reviewed and appropriate material
will be referenced.  A planning meeting was held to scope out and generate an outline identifying elements  that
will be addressed in the Issue Paper. This outline was completed and reviewed by the Engineering Forum.  During
the 1st Quarter, FY 94 an initial draft of the issue  paper  was completed. The draft issue paper was provided to the
Engineering Forum for review. The TSC addressed the Forum's  comments, and prepared the document for peer
review.  The document has been peer reviewed and  is currently being finalized for publication.
                                                 37

-------
                                          ISSUE PAPER
Project Name: Open Burn/Open Detonation Site Characterization
Site:Open Burn/Open Detonation
Site ID:

Type-Lead:
Requested by: Groundwater Forum/Federal Facilities
Lead Scientist: Alan Crockett (208) 526-1574

Start Date: March 1995
Expected Completion Date: December 1995
Revised Completion Date:
Estimated Budget: 525,000
Revised Budget:SO
Major Contaminants: Explosives
Total Expenditures: $6,373
Total FY95 Expenditures: S6,373
Total 3rd Qtr. Expenditures: S3,133
There are over 100 RCRA Facilities that are regulated under Subpart X.  These sites are required to have
groundwater exposure assessments, and establish groundwater monitoring systems. Approximately 90% or more
are Open Burning/Open Detonation (OB/OD) facilities.  Besides RCRA facilities, there are CERCLA sites across
the Nation that are currently being investigated, especially for base closure, that will  also have similar explosive
problems.

The EMSL-TSC is obtaining available information concerning the sampling methods, monitoring approaches and
analytical protocols for  addressing the characterization of these contaminants. Following the assessment of
available data the  CRD-LV  TSC prepared  a suggested outline that identifies  the major elements that will be
addresses in the Issue Paper. The Federal Facilities Forum has suggested that an  Issue  Paper addressing a different
source of explosive contaminants be developed. The TSC will respond to this request when received.
                                                 38

-------
                                        COORDINATION
Project Name: Superfund Coordination
Site: Superfund Coordination
Site ID:                                                    Job Order No: 226 10101

Type-Lead:
Requested by: Ken Brown
Lead Scientist: Phil Malley

Start Date: On-going October 1991
Expected Completion Date: September 1995
Revised Completion Date:

Estimated Budget: 5100,000                         Total Expenditures: $497,055
Revised Budget: S                                 Total FY95 Expenditures: 584,844
Major Contaminants: N/A                          Total 3rd Qtr. Expenditures: 528,773


This project provides for Superfund coordination of requests received by the Technology Support Center and
implementated when assigned to the off-site contractor. Activities include preparation of reports and tracking of
projects, and documenting costs.


Project  Name:  RCRA Coordination
Site: RCRA Coordination
Site ID:                                                    Job Order No: 226 10601

Type-Lead: Ken Brown
Requested by: Phil Malley
Lead Scientist:

Start Date: On-going October 1991
Expected Completion  Date: September 1995
Revised Completion Date:

Estimated Budget: 540,000                          Total Expenditures: S57.710
Revised Budget: 5100,000                           Total FY95 Expenditures: 55,116
Major Contaminants: N/A                          Total 3rd Qtr. Expenditures: 57

This project provides for RCRA coordination of requests received by the Technology Support Center and
implementated when assigned to the off-site contractor. Activities include preparation of reports, tracking of
projects, and documenting costs.
                                                39

-------
                                   TECHNOLOGY TRANSFER


Project Name: Superfund Technology Transfer
Site: Superfund Technology Transfer
site ID:                                                    Job Order No: 224 10020

Type-Lead:
Requested by: Director TSC
Lead Scientist: Clare Gerlach

Start Date:
Expected Completion Date:
Revised Completion Date: September 1995

Estimated Budget: 580,000                          Total Expenditures: S 70,690
Revised Budget: S                                 Total FY95 Expenditures: S 70,690
Major Contaminants:                              Total 3rd Qtr. Expenditures: $21,405

One of the objectives of the CRD-LV TSC is to identify and make available CRD-LV measurement technologies
that are applicable for characterizing contaminants. Documenting the adequacy of these technologies, the
application and  their identity requires the development of case studies, fact sheets, demonstrations and workshops.
During this quarter a case study identifying the sampling/monitoring and analytical methods that were used to
characterize mercury contamination at Oakridge was submitted  for printing.  In addition, several one-page fact
sheets and two four-page fact sheets were developed.  The two four-page fact sheets are titled, "EPA Training
 Programs Available Through the CRD-Las Vegas", and "Robust Statistical Intervals for Performance Evaluation."
                                                 40

-------